-------
TABLE VIII-5
MANUALLY OPERATED PHYSICAL-CHEMICAL PRETREATMENT SYSTEMS
CAPITAL COSTS
Wastewater Generated
liters/day
(gallons/day)
Tanks (plastic)
Mixers (portable)
Pumps
Piping, Valving .
Material Handling Equipment
Subtotal
Electrical
Freight and Installation !
Contingency
Total
115
(30)
$ 95
700
600
700
250
$2,345
235
1,290
580
$4,450
300
(80)
$ 455
700
600
875
300
$2'>930
295
1,615
725
$5,565
107
-------
TABLE VIII-6
MANUALLY OPERATED PHYSICAL-CHEMICAL PRETREATMENT SYSTEMS
OPERATING COSTS
Wastewater Generated
liters/day
(gallons/day)
115
(30)
300
(80)
Depreciation
Labor - direct
Labor - indirect
Chemicals
Polymers
Acid
Inorganic salt
Power
Maintenance
Sludge Disposal
POTW user charge
Monitoring
Total
$ 790
4,000
800
$ 985
4,000
800
3
15
25
150
135
340
35
1,200
8
40
60
150
165
900
90
1,200
$7,500
$8,400
108
-------
VII1-7
WASTEWATER DISPOSAL BY CONTRACT HAULING
CAPITAL COSTS
Waste-water Generated
liters/day
(gallons/day)
Holding Tank ;
Piping and Valving ;
Subtotal
Electrical and Instrumentation
Engineering, Freight and Installation
Contingency
/ Total ' :
Square Meters (feet) Required
Additional Utility Building (if required)
110
(30)
$1,000
500
11,500
150
825
375
$2,900
5(50)
$2>000
300
(80)
$2 , 100
1,050
$3,150
315
1,735
780
$6,000
,5(50)
$2 , 000
950
(250)
$5,000
2,500
$7,500
750
4,100
1,900
$14,250 ,
12(125)
$ 4,000
109
-------
TABLE VIII-8
WASTEWATER DISPOSAL BY CONTRACT HAULING
OPERATING COSTS
Wastewater Generated ;
liters/day
(gallons/day)
Depreciation 1
Labor - direct j
Labor - indirect :
Maintenance
Sludge Transportation & Disposal
Total
,110
(30-)
$ 515
2,000
400
90
2,250
$5,255
300
(80)
$1,065
2,000
400
180
6,000
$9,645
950
(250)
$2,500
2,000
400
400
18, 750
$24,050
110
-------
cn
1
1— i
f—l
>
w
CQ
rij
EH
--«
o m
m i >
C fl ctj
- (j^ ^3 ^j
U \\
W CQ
M S-l C
0 CD O
-P -P r-l
flj -H r-<
3 r-l (tj
(U cn
•P '—
cn
a
S
o ; o o o m o m
o o o m f- o CN
o - in m o P- vo o>
r* i m o r-i in CN cn
«H r-l
{/> l
I
j
o o o o in o in
o o o in 'P» o CN
o in in o P» vo cn
p» rno«-»incicn
' rH r-i
^ ^
1
1
- |
f
|
•
•
o ! o o o in o in
o o o m r- o r>i
o ' in m o r^* v^ cn
p^ (**) o *-H in CM cn
\ ' . -
G
O
3 ; f-H
CQ i ,H
cn • . fl
CD -P
s-i ; en
CU C
: H -
•.
03-^; T3
S-4 CQ i CO C
O CU CD nJ
-P >H 03
O N O CT>
S N ! K fi
O ! -H
J3 G CD M
-P 1 iH CD
•H T3 [ jQ CD
3 C -H . C
— fU ! X r-l -H
, cu ^ <8 cn
£ - r-l 4J C f >1
CDCQfa O^&3 Or-(
-P M I -P (d C 03
cnoi'-a A o - cu -P
>i-P ! 3 -H 4J Cn O
cn«J cncn s-i je • G EH
r-i ' c -P cn -H
Oi 3 ! -H O -H 4J
S en a CD CD C
3 0) -H r-i iH O
eu M &i pa fci o
111
-------
NONWATER QUALITY ASPECTS j
Energy I
The energy use associated with physical-chemical treatment was
presented in the preceding section for each model plant size. On an
industry-wide basis, if all j plants with a wastewater discharge
installed P-C treatment systems, the total energy use would be
approximately 0.5 to 1.5 MkWh/yr. This assumes that all plants
currently discharging no wastewater will continue to do so. No
additional credit was allowed for any systems which may already be in
place. Contract hauling woiild not involve major additional, energy
expenditures by the ink industry.
i •
Sludge Quantity and Characteristics
P-C treatment is not widely used by the ink industry, and EPA did not
collect samples of ink sludges. If the entire industry were to
install P-C treatment systems, ;the Agency estimates that 14,000' liters
(3,600 gal) of sludge would be 'produced daily. This sludge would most
likely have the same toxic pollutants as untreated ink wastewater, but
at higher concentration. Untreated ink wastewater characteristics are
listed in Table V-15. i
If the entire wastewater volume of the ink industry is contract
hauled, the toxic pollutant | loading would equal that presented in
Table V-18 (2.2 kg/d of organic toxic pollutants and 19 kg/d of
inorganic toxic pollutants). Reduction of wastewater volume by high
pressure rinse alone, without any other dry clean up procedures, will
not affect the amount of polliitants discharged from the ink industry,
but it can significantly reduce the wastewater volume and the disposal
costs for plants that contract haul any of their wastewater.
r ,- ,.
Solvent-Wash Subcategory \
i
Currently the only unregulated .segment of the solvent-wash subcategory
of the ink industry is the existing source indirect dischargers. A
key point in favor of the no discharge regulations for the remaining
segments of this subeategory was the proven cost effectiveness of on-
site solvent recovery versus outside purchase of reclaimed solvent.
j . .
I •
The July 1975 Development Document stated that the in-house cost of
reclaiming solvents was 1.0 to 13.80/1 (3.6 to 14.20/gal) , while the
selling price of reclaimed solvents was 10 to 300/1 ($.40 to $l/gal).
These costs compared favorably with the cost of purchasing new
solvent. I
The Agency updated these data with a telephone survey of ink plants
using recovered solvent for tubi cleaning.
112
-------
Corvsiderirxg the rising costs of labor, energy, and sludge disposal, in
1979, solvents can be reclaimed for 5.4 to 8.50/1 (200 to 300/gal),
while reclaimed solvents are selling for 110/1 (450/gal) to well over
300/1 ($l/gal) . New solvents generally cost over 300/1 ($l/gal).
113
-------
-------
SECTION IX
EFFLUENT REDUCTION ATTAINABLE THROUGH THE APPLICATION OF
THE BEST AVAILABLE TECHNOLOGY ECONOMICALLY ACHIEVABLE
EFFLUENT LIMITATIONS GUIDELINES
INTRODUCTION
EPA determines the effluent limitations that must be achieved by July
1, 1984, by identifying the vejry best control and treatment technology
employed by a specific point source within the industrial category or
subcategory or by one industry where it is readily transferable to
another. The Agency must specifically determine the availability of
control measures and practices to eliminate the discharge of
pollutants, taking into account the cost of such elimination.
Consideration also was given to:
o The age of the equipment and facilities;
o The processes employed;
o The engineering aspects of the application of various types
of control techniques;
o Process changes; and '
o Nonwater quality environmental impact (including
requirements). '
energy
The Best Available Technology Economically Achievable (BAT) emphasizes
in-process controls as well! as control or additional treatment
techniques employed at the end of the production process. It
considers those plant processes and control technologies which, at the
pilot plant, semi-works, •and other levels, have demonstrated
sufficient technological performances and economic viability to
justify investing in such facilities. BAT represents the highest
degree of demonstrated control technology for plant-scale operation up
to and including '?no discharge" of pollutants. The costs' of this
level of control are defined top-of-the-line current technology,
subject to limitations imposed by economic and engineering
feasibility. There may be some technical risk, however, with respect
to performance and certaintyi of costs. Therefore, some process
development and adaptation may be necessary for application at a
.specific plant site.
115
-------
The statuatory asgegsment of !BAT "consi
a alnc^g of costs againstL
"
In developing the proposed BAT,
however, EPA has given substantial weight to the reasonableness of
costs. The Agency has considered the volume and nature of discharges, •
the volume and nature of discharges expected after application of BAT,
the general environmental effects of the pollutants, and the costs and
economic impacts of the required pollution control levels.
Despite this expanded consideration of costs, the primary determinant
of BAT is effluent reduction capability. As a result of the Clean
Water Act of 1977, the achievement of BAT has become the principal
national means of controlling jtoxic water pollution. EPA has selected
BAT technology which will significantly reduce this toxic pollution.
i ' ;
IDENTIFICATION OF BAT TECHNOLOGY
Both in-plant and end-of-pipe modification are necessary for most
plants to achieve BAT. Control technologies are discussed in detail
in Section VII while costs a!nd operating parameters for model plants
are given in Section VIII. i
The Agency considered the following technologies:
In-Plant Controls !
wastewater reduction -through high pressure water washing of
equipment, dry floor clean-up and sealing of floor drains,
and use of squeegees jprior to tank cleaning-
- wastewater reuse through recycle of caustic rinses back into
caustic tank as majke-up and water rinses back into the
product or rinse water.
I
End-of-Pipe Controls ;
Physical-chemical treatment including coagulation/precipitation
and sedimentation i
- Biological treatment iby aerated lagoons
Contract hauling | i
- Evaporation
Ultrafiltration |
Reverse osmosis ' j : ;
Activated carbon adsorption
Technology Options Available i
I (
Option One - Physical-chemical treatment (coagulation/^precipation) and
sedimentation) ;
116
-------
Option Two - Elimination of pollutant discharge through the use of
contract hauling of nonrecyclable wastes.
Other evaluated technologies were unacceptable due to a lack of
demonstrated effectiveness on ink wastewater or severe economic or
nonwater quality impacts. j
t
Rationale Used to Develop BAT Effluent Guidelines
Based on analysis of available: control options, the Agency selected
Option Two for the Caustic and/or Water-Wash Subcategory. The amount
of wastewater generated by all ink plants is sufficiently small in
volume to be contract hauled to hazardous waste disposal facilities.
Strict control of water use through in-plant controls such as high
pressure rinses •and recycle of water and caustic washes, can reduce
wastewater generation from ink1 plants significantly.
The remaining wastewater should be sufficiently small in volume to
make contract hauling practical and eliminate any need for discharge.
However, the basis of the analysis for BAT was contract hauling of
1005? of wastewater currently generated. This was due to the fact that
many plants produce water rinsed ink in batches as small as five
pounds. Due to the relatively;small volumes of water produced by ink
plants, EPA .assumed that most plants would choose to contract haul all
wastes rather than attempt recycle or other in-plant controls.
The Agency rejected Option One because it fails to provide consistent
removal of toxic pollutants to the level attained by Option Two. High
concentrations of toxic pollutants have been measured in the effluents
from plants using the best end-of-pipe technologies. Due to the toxic
nature of ink manufacturing wastewater, the Agency has determined that
disposal'of these wastes to prbperly designed hazardous waste disposal
sites is preferable to discharge to surface waters.
The most significant conventional pollutants and pollutant parameters
controlled are BOD, TSS, oil and grease, and pH.
Sizeff Age, Production
Cleaning Techniques
Methods, Raw Materials and Products, Tub
Ink production uses process i equipment which has not changed
appreciably for many years. This equipment produces ink in batches of
varying sizes. Therefore the age of a plant has little bearing on its
waste characteristics. Size: of a plant affects only the volume of
wastewater produced. Raw matefials used and products produced affect
wastewater characteristics only to the extent that they affect
equipment cleaning techniques. These techniques are the basis of
subcategorization of the industry.
117
-------
In summary, the factors of; size, age, production methods, raw
materials, and products are noip significant to effective application
of the control technology. ! Detailed discussion of the wastewater
characteristics for the ink industry is available in Section V.,
Engineering Aspects of Best
Achievable
Available Technology Economically
The effectiveness of in-plant controls has been described in detail in
Section VII. Of the plants using a water rinse, 12 report that they
generate no wastewater.
High pressure washing generally can reduce wastewater generation by
90%. Elimination of floor |drains and subsequent dry clean up of
spills, and use of squeegees or rags for precleaning of equipment can
further reduce wastewater generation. The applicability of in-plant
controls is dependent on the types and quantities of water rinsed ink
produced. Plants which only Occasionally produce water rinsed ink or
make very small batches may not find in-plant controls to be cost-
effective. '
Simple volume reduction does not also reduce pollutant mass. It does
concentrate pollutants in manageable volumes of water which then can
be recycled back into product or contract hauled to hazardous waste
disposal facilities. If wastewater can be recycled, valuable raw
materials are reclaimed.
Nonwater Quality Environmental Impact
I :
EPA anticipates, based on information transferred from its paint
industry study, that the implementation of BAT at a plant will
generate up to 0.2 liters of I hazardous waste per liter of caustic or
water-washed (water rinsed) ink produced. Ink_TpJLan±J
^
Jb:cea±ment^-^^ WJj-1 increase the
reduce the sludge component: as facilities adopt in-plant control
alternatives to physical-chemical treatment.No significant change in
consumptive water use or atmospheric quality in terms of air
emissions, noise, or radiationj will result from implementation of BAT.
i
Negligible amounts of energy will be used for pumping, mixing, and
contract hauling of these wastes.
Total Cost of Application in Relation to Effluent Reduction Benefits
i ' :
Based on the cost information in Section VIII the total investment and
annualized costs are estimated' to be negligible due to the nature of
118
-------
current direct discharge by the ink industry. No ink plants
discharge directly to surface water. BAT limitations are being issued
to provide guidelines for current indirect dischargers who convert to
direct discharge. No closures in the ink industry are expected as a
result of the proposed limitations.
BAT EFFLUENT GUIDELINES •'.
There shall be no discharge of pollutants in process wastewaters from
the Caustic and/or Water-Wash Subcategory of the Ink Formulating Point
Source Category. The prohibition of discharge of pollutants from the
Solvent-Wash Subcategory promulgated in HO CFR 447 on July 28, 1975,
remains unchanged. j .
REGULATED POLLUTANTS !
Issuance of this regulation will prevent discharges of all pollutants
from affected ink plants. The significant toxic pollutants controlled
are:
Chromium (Total)
Copper (Total)
Lead (Total)
Zinc (Total) ;
1,1,1-Trichloroethane
1,2-Diphenylhydrazine
Methylene Chloride
Isophorone
Ethylbenzene
Pentachlorophenol
Di(2-ethylhexyl) Phthalate
Toluene
Di-n-octyl Phthalate
Tetrachlorethylene
Trichloroethylene
119
-------
-------
SECTION X
NEW SOURCE PERFORMANCE STANDARDS
INTRODUCTION
The basis for New Source Performance Standards (NSPS) under Seqtion
306 of the Act; is the best available demonstrated technology. New
plants have the opportunity to design the best and most efficient ink
manufacturing processes and , wastewater treatment technologies, and
Congress therefore directed EPA to consider the best demonstrated
processes and operating methods, in-plant control measures, end-of-
pipe treatment technologies, and other alternatives that reduce
pollution to the maximum extent feasible, including, where
practicable, a standard permitting no discharge of pollutants.
IDENTIFICATION OF NEW SOURCE PERFORMANCE STANDARDS
New Source Performance Standards rest on the technology options
considered for BAT in Section IX. Since BAT represents the current
state-of-the-art technology, no further improvement for new sources is
possible. Based on analyses of the technology options EPA selected
BAT Option Two for NSPS for the Caustic and/or Water-Wash Subcategory.
This option completely removes pollutants from ink plant discharges.
Selection of BAT Option One would provide less stringent requirements
for NSPS than BAT. This would be inconsistent with the basis for
NSPS. - :
Rationale Used to Develop NSPS;Effluent Limitations
The rationale used to select NSPS was identical to that used to select
BAT in section IX. No justification could be found for selecting a
technology option for NSPS less stringent than BAT.
Size, Production Methods,, Raw Materials and Products, Tub Cleaning
Techniques I
The aspects of size, production methods, raw materials, and products,
and tub cleaning techniques for the ink industry discussed for BAT in
Section IX also apply to NSPS.. '
Engineering Aspects of New Source Performance Standards
In addition to the engineering aspects discussed in Section IX for
BAT, it should be noted that the design of new plants offers the
opportunity to optimize performance of in-plant controls. This
optimization should enable new plants to attain NSPS with reduced
Hazardous waste generation in comparison with many existing plants
meeting BAT. ;
121
-------
Nonwater Quality Environmental! impacts
I
The nonwater quality environmental impacts associated with NSPS
effluent limitations are the :same as those associated with BAT
effluent limitations, as discussed in Section IX. The energy
requirements to meet this standard should represent a small fraction
of the plants* consumption. \ [
[ i , , , r ,m „ , i ., _ i
Total Cost of Application in Relation to Effluent Reduction Benefits
I ,
At this time, 40 percent of; all plants in the industry are indirect
dischargers; the remaining 60 ! percent practice no discharge., The
Agency expects that the majority of new firms entering the industry
will be no dischargers or indijrect" dischargers. EPA does not expect
any significant impacts. i
NSPS EFFLUENT LIMITATIONS
There shall be no discharge ojf pollutants in process' waste waters from
the Caustic and/or Water-Wash (Subcategory of the Ink Formulating Point
Source Category. [
i
The prohibition of discharge i of pollutants from the Solvent-Wash
Subcategory promulgated in !40 CFR 446 on July 28, 1975, remains
unchanged.
REGULATED POLLUTANTS
The pollutants controlled are [identical to those controlled by BAT and
discussed in Section IX. >
122
-------
SECTION xi
PRETREATMENT STANDARDS FOR EXISTING SOURCES
INTRODUCTION :'.....
The effluent limitations that must be achieved by existing sources in
the ink industry that discharge into a publicly owned treatment works
(POTW) are termed pretreatment standards. Section 307 (b) of the Act
requires EPA to promulgate pretreatment standards for existing sources
(P'SES) to prevent the discharge of pollutants that pass through,
interfere with, or are otherwise incompatible with the operation of
POTW. The Clean Water Act of 1977 adds a new dimension by requiring
pretreatment for: pollutants,: such as heavy metals, that limit POTW
sludge management alternatives, including the beneficial use of
sludges on agricultural lands. The legislative history of the 1977
Act indicates that pretreatment standards are to be technology-based,
analagous to the best available technology for removal of toxic
pollutants. The general pretreatment regulations (40 CFR Part 403),
which served as the framework for these proposed pretreatment
regulations for the ink industry, can be found at 43 FR 27736-27773
(June 26, 1978) .
Consideration was also
pretreatment standards:
given to the following in establishing the
o Plant size, age of j equipment and facilities, production
methods, raw materials and products, tank cleaning
techniques;
The engineering aspects of the application
technology and its relationship to POTW;
of pretreatment
o Nonwater quality environmental impact (including energy
requirements); and
o The total cost of.application of technology in relation to
the effluent reduction and other benefits to be achieved from
such application. !
Pretreatment standards must reflect effluent reduction achievable by
the application of the best available pretreatment technology. This
may include primary treatment technology as used in the industry and
in-plant control measures when such are considered to be normal
practice within the industry- ;
A final consideration is the determination of economic and engineering
reliability in the application of the pretreatment technology. This
123
-------
must be determined from the results of demonstration projects, pilot
plant experiments, and most preferably, general use within the
industry. |
1 ! ' ' ;
IDENTIFICATION OF PRETREATMENTi STANDARDS '••
Ink plants discharge almost exclusively to POTW. Less than 15% of the
plants use some pretreatment technologies and 13% practice in-plant
controls to reduce wastewater generation. The technologies considered
for pretreatment are identical to those considered for BAT in Section
IX with the exception of solvent reclamation which was considered for
solvent-wash inks. Analysis! of the technologies resulted in the
development of two options forl pretreatment standards for existing
sources.
Technology Options Available: '
\
Option One - Physical-chemical; treatment by coagulation/flocculation
and sedimentation- (BAT Option One)
Option Two - No discharge of pbllutants through the use of
contract hauling of nonrecyclable wastes
(BAT Option Two) j
Other evaluated technologies were unacceptable due to a lack of
demonstrated effectiveness on ink wastewater, or severe economic or
nonwater quality impacts. !
Rationale Used to Develop P re treatment Standards for Existing Sources
The elimination of pollutantI discharge for solvent-wash ink is based
on the hazardous and toxic nature of these wastes and the economic
advantage in reclaiming thej solvents. Since no water is used in
cleaning solvent-wash equipmen-b, the solvents and off~specification
batches comprise the entire! discharge of this subcategory. Most
plants in the subcategory currently meet no discharge. The Agency is
requiring that the remainder;of the industry meet this level of good
practice.
As in BAT, caustic or water-wash subcategory pretreatment standards
are based on contract hauling of all wastewater generated,. It is
possible to reduce waste generation through the use of in-plant
controls such as high pressure rinses, recycle of water and caustic
washes. The Agency rejected Option one because they fail to provide
consistent removal of toxic pollutants to the level attained by Option
Two. Djifi,,. ta__-the_J-oyic naiuijce—of-—iink—was-tewateg?—EPA-teas~xLejbermined
ihat. the disposaljQ_f_J^ege-4(iasjies--±^o__BrjiT3erlv designed hcizardous waste
'disposal sites ispref erable
124
-------
Size,
Product, ion Methods, Raw Materials and Products, Tub
Cleaning Techniques
. t ." ' '
As previously noted in Section IX for BAT, ink is produced with
methods and equipment which are relatively uniform from plant to
plant. As a result, the factors of size, age, production methods, raw
materials and products do hot affect wastewater characteristics
significantly. Tub cleaning techniques are the fundamental factors
which control these characteristics. Therefore, the subcategorization
of the ink industry is based! on use of solvent, caustic or water for
tub cleaning. ' • -'
Engineering Aspects of Pretreatment for Existing Sources
Waste solvents produced by tub and equipment cleaning can be
regenerated easily through Distillation. Not surprisingly, many
plants recover their solvents and distill them on site. Other plants
sell waste solvents to scavengers who regenerate and market them. Few
plants therefore have any reason to discharge waste solvents to the
POTW.
As noted in Section IX for BAT, the use of in- plant controls
significantly reduces wastewater from caustic and/ or water -washed ink
formulation which must be eliminated™
Recycle, high pressure rinses,; dry clean up of floors, and precleaning
of tubs with squeegees or rags are all techniques to reduce wastewater
for disposal to 0.2 liter/liter or less. The removal of the non-
recyclable wastes by contract hauler to a hazardous waste disposal
site should provide an acceptably safe method of disposal for these
toxic materials. Recycle of wastewater to the product conserves raw
materials in addition to saving water.
- { . .
Nonwater Quality Environmental Impacts
EPA estimates that the implementation of PSES will generate an
additional 23,000 metric tons (wet) of hazardous wastes. I± should_be
noted that — PSES also__jwill commensurately reduce concentrations and
These sludges will
become — more
_
polluTants in POTW sludges.
arrrerncri3±-e
to
-£pssibly_ including beneficial use on agricultural lands. Moreover,
disposal of adulterated POTW: slud^s"TsrsTgnTFicantlY more" diff icuTt
and costly — than. — djuspnsaJ - of — _£ „ wasjtas— . _£rom
individual plant sites.
No significant change in consumptive water use or atmospheric quality
in terms of air emissions, noise, or radiation will result from
implementation of ;PSES.
125
r S4-3L
o
-------
Total Cost, of Application in Relation to Effluent Reduction Benefits
Based on the cost information presented in Section VIII, elimination
of pollutant discharges by ink'plants to POTW is possible with a. total
capital investment of 1.5 million dollars. The annualized cost for
the industry will be 3.0 million dollars.
PRETREATMENT STANDARDS FOR EXISTING SOURCES
There shall be no discharge
the Solvent-Wash Subcategory
of the Ink Formulating Point
of
and
S6urce
REGULATED POLLUTANTS
Issuance of this regulation
pollutants from affected
toxic pollutants controlled are
Chromium (Total)
Copper (Total)
Lead (Total)
Zinc (Total)
1,1,1-Trichloroethane
1,2-Diphenylhydrazine
Methylene Chloride
Isophorone
will prevent the discharges of all
indirect dischargers. The most significant
pollutants in process wastewaters from
the Caustic or Water-Wash Subcategory
Category.
Ethylbenzene
Pentachlorophenol
Di (2-ethylhexyl) Phthalate
Toluene
Di-n-octyl Phthalate
Tetrachlorethylene
Trichloroethylene
If the Agency had selected Pretreatment Option One for the caustic
and/or water-wash subcategory, numerical mass limitations would be
used. Concentration values arfe not appropriate due to the ease with
which dilution can occur by indiscriminate water use in equipment
cleaning. '
The mass limitations are basedi on the median percent removal observed
in the paint industry, average observed pollutant concentration in
untreated wastewater reported in Table V-15, and wastewater discharge
of 0.2 liter per liter ofj water rinsed ink produced. Since no
operating precipitation systemjs were found in the ink industry, it was
necessary to transfer the performance of this treatment option from
the paint industry. Both industries have similar wastewaters.
126
-------
The resulting daily maximum mass limitations would be:
Pollutant
Chromium (Total)
Copper (Total)
Lead (Total)
Zinc (Total)
1,1,1-Trichloroethane
Ethylbenzene
Di (2-ethylhexyl)Phthalate
Tetrachloroethylene
Toluene
Trichlorpethylene
mg/1000 liters
water rinsed
ink
3240
1060
3021
82
16
166
75
5
84
67
lb/1000 gallons
water rinsed
jnk
0.02710
0.00890
0.02520
0.00070
0.00020
0.00140
0.00060
0.00004
0.00070
0.00060
127
-------
-------
SECTION XII
PRETREATMENT STANDARDS FOR NEW SOURCES
INTRODUCTION ;
Section 307(c) of the Act requires the EPA to promulgate Pretreatment
Standards for New Sources (PSNS) at the same time that it promulgates
NSP3. New indirect dischargers, like new direct dischargers, have the
opportunity to incorporate the best available demonstrated
technologies including process changes, in-plant controls, and end-of-
pipe treatment technologies, and to use plant site selection to insure
adequate treatment system installation.
IDENTIFICATION OF NEW SOURCE PRETREATMENT STANDARDS
New Source Pretreatment Standards were based on the options considered
for PSES in Section XI. Since PSES represents the current state-of-
the-art technology, no further improvement for new sources is
possible.
Based on analyses of the technology options, EPA chose PSES Option Two
for PSNS for the caustic and/or water-wash subcategory. This option
completely eliminates pollutant discharges from ink plants to POTW.
Selection of PSES Option One would provide less stringent requirements
for PSNS than PSES and would be inconsistent with the basis for PSNS
limitations.
Rationale Used to Develop PSNS Effluent Limitations
i
The rationale used to select PSNS was in fact identical to that used
to select PSES in Section XI. : No justification could be found for
selecting a technology option ifor PSNS less stringent than PSES.
Size, Production Methods, Raw Materials and Products, Tub Cleaning
Techniques
The aspects of size, production methods, raw materials and products,
and tub cleaning techniques for the ink industry discussed for PSES in
Section XI also apply to PSNS.i
Engineering Aspects of New Source Performance Standards
In addition to the engineering aspects discussed in Section XI for
PSES, it should be noted that the design of new plants offers the
opportunity to optimize performance of in-plant controls. This
optimization should enable new plants to attain PSNS with reduced
129
-------
hazardous waste generation in comparison to many existing plants
meeting BAT. '•
i
Nonwater Quality Environmental I Impacts
( . • , :
The nonwater quality environmental impacts associated with NSPS
effluent limitations are th4 same as those associated with PSES, as
discussed in Section IX, Energy consumption in order to attain new
source performance should represent a negligible fraction of total
plant consumption. .
Total Cost of Application in Relation to Effluent Reduction Benefits
i
Based on the cost information in Section VIII, EPA estimates that the
complete elimination of pollutants in new source process wastewater
indirect discharges may add 0.. 6 cents per pound to the price of ink.
i , i
PRETREATMENT STANDARDS FOR NEW SOURCES
There shall be no discharge of pollutants in process wastewaters from
the Caustic and/or Water-Wash Subcategory of the Ink Formulating Point
Source Category.- i
The prohibition of discharge of pollutants from the Solvent-Wash
Subcategory promulgated in 40 CFR 446 on July 28, 1975 remains
unchanged.
REGULATED POLLUTANTS •
The pollutants controlled are identical to those controlled by PSES
and discussed in Section xt- if the Agency had selected pretreatment
Option One for the Caustic ^ncl/or Water-Wash Subcategory, numerical
mass limitations equal to thos^ calculated for this option in Section
XI would have been used.
130
-------
SECTION XIII
AC KNOWLEDGMENTS
Acknowledgment is made to all Environmental Protection Agency
personnel contributing to the'overall project effort. Specifically,
the development of this report was under the direction of the
following EPA personnel:
Robert B. Schaffer
John E. Riley
James R. Berlow
Lisa Friedman
Barry Malter
Louis DuPuis .
John Kukulka
Chris Ehret
Director, Effluent Guidelines Division
Chief, Wood Products & Fibers Branch
Project Officer, Paint & Ink Industries
Office of General Counsel
Office of General Counsel
Office of Analysis & Evaluation
Office of Analyisis & Evaluation
Monitoring & Data Support Division
Acknowledgment is also made for the helpful cooperation
following paint and ink industry Working Group members:
of the
Michael Flaherty
Ronald Turner
Richard Raines
Fanny Knox
Roman Kuchkuda
Benjamin Lim
Matthew Straus
Special thanks go to David Alexander, the EPA Project Officer for the
for the first two years of the project, and to the . Document
Preparation Staff of Kaye Starr, Pearl Smith, Nancy Zrubek, Vicky
Wilson, and.Carol Swann. Micki Treacy is especially noted for her
valuable secretarial assistance.
Appreciation is extended toithe National Association of Printing Ink
Manufacturers especially Executive Director, James E» Renson, and the
National Printing Ink Research Institute for their extremely valuable
assistance and cooperation throughout this project.
Appreciation is also extended to the
participation in the study: <
A.J. Daw Printing Ink Co.
Braden Sutphin Ink Co. '
Capitol Printing Ink Co., Inc.
Colonial Printing Ink Div. , U..S.P.
Inmont Division Carrier Corp,
Morrison Printing Ink Co.'
Richardson Ink Co. I
following companies for their
131
-------
Roberts and Porter, Inc.
Sun Chemical Corp. '
The following members of the Burns and Roe Technical Staff made
' of
significant contributions to th'e project and the
report: I
development
the
Arnold S. Vernick, P.E.
Howard D. Feiler, P.E.
Paul J. Storch, P.E.
Mark V. Sadowski
Richard Hergenroeder
Roy E. Ehlenberg
Manager, Environmental Eng.
Prjoject Manager
Project Engineer
Assistant Project Eng.
Cijvil Engineer
Systems Engineer
The assistance of Mrs. S. ijrances Thompson and Miss Emilie Carl of
Burns and Roe in the typing of jthis report is specifically noted.
The efforts of Edward H. Richardson Associates, Inc. in regard to
sampling and analysis is greatly appreciated. Specifically, the
efforts of Mr. Albert Merena are acknowledged.
132
-------
SECTION XIV
; REFERENCES
1. Environmental Protection Agency, Development Document for Effluent
Limitations Guidelines and New Source Performance Standards for the
011 Base Solvent Wash Subcategories of the Paint and the Ink
Formulating Point Source Category, Washington, DC, July 1975.
3
2. Burns and Roe Industrial Services Corporation, Draft Development
Document for Effluent Limitations Guidelines. Pre treatment Standards
and New Source Performance Standards for the Paint and Ink Formulating
Point Source Categories - Water- Base, Water-Wash, and Caustic-Wash
Subcategories. Paramus, NJ, September, 1976. --
3. Arthur D. Little, Inc. "Economic Analysis of Proposed Effluent
Guidelines: Paint and Allied Products and Printing Ink Industries",
Draft Document for the Environmental Protection Agency, Washington
DC, August, 1974. i
4- Printing Ink Handbook, 3rd Edition, National Association of
Printing Ink Manufacturers, Inc., Harrison, NY, 1976,.
5. Shreeve, R. , "Surface-Coating Industries", Chemical Process
Industries, 3rd Edition, McGraw-Hill Book Company, New York, NY, 1967.
6- "Census of Manufactures", Bureau of the Census, U.S. Department of
Commerce, 1972.
• " • ' I .
7. Raw Materials Data Handbook - Organic Solvents, National Printing
Ink Research Institute, Lehigh University, Bethlehem, PA, 1974.
8 Raw Materials Data Handbook - Plasticizers, National Printing Ink
Research Institute, Lehigh University, Bethlehem, PA, 1975.
9- Colour Index, 3rd Edition, Society of Dyers and Colourists with
acknowledgement to the American Association of Textile Chemists and
Colorists, 1971.
10. Nie, N., C. Hull, J. /Jenkins, K. Steinbrenner, D. Bent,
Statistical Package for the Social Sciences , 2nd Edition, McGraw-Hill
Book Company, 1975,.
11. Environmental Protection Agency, "Field Notes and Chemical
Analyses - Survey of Paint and Ink Manufacturers in Oakland,
California," collected by National Field Investigations Center,
Denver, Colorado, October, 1973.
133
-------
12. Environmental Protection Agency, Development Document for Prop.Qg_ed
Effluent Limitations Guidelines and New Source Performance Standards
for the Synthetic Resins Se'qment of the Plastics and Synthetic
Materials Manufacturing Point Source Category, Washington, DC, August,
1973, | • '
13. Reid, L.C., "Memorandum to Record," (Specifying Plants Attaining
No Discharge of Process Wastewater to Surface Waters), National Field
Investigations Center, Environmental Protection Agency, Denver,
Colorado, December, 1973-January, 1974.
14. Reid, L.C., and A. Masse, "[Trip Reports," (Paint and Ink Plants in
Chicago, Illinois and Oakland, California Areas), National Field
Investigations Center, Environmental Protection Agency, Denver,
Colorado, December, 1973-January, 1974.
i
15. "Water Quality Criteria, 19;72," National Academy of Sciences and
National Academy of Engineering for the Environmental Protection
Agency, Washington, DC, 1973 (U.S. Government Printing Office Stock
No. 5501-00520). | '
16. Williams, Alex, "Printing jinks," Noyes Data Corporation, Park
Ridge, NJ, 1972.
17. King, Robert, "Trip Report,'" National Field Investigations Center,
Environmental Protection Agency, Denver, CO, November,! 1973.
18. Enviornmental Protection | Agency,
Handbook for Monitoring
Industrial Wastewater, Washington, DC, August, 1973.
—'-"•-••-- — - ----"' I
19. Environmental Protection Agency, Methods for Chemical Analysis of
Water and Wastes, Cincinnati, OH, 1974.
20. Environmental Protection Agency, Federal Guidelines: State
Local Pretreatment Programs, Washington, DC, January, 1977.
and
21. Environmental Protection Agency, Rationale for the Development of
BAT Priority Pollutant Parameters, Washington, DC, June, 1977.
22. Environmental Protection Agency, Sampling and Analysis Procedures
for Screening of Industrial Effluents for Priority Pollutants,
Cincinnati, OH, April, 1977.. :
23. Environmental Protection (Agency, General Reference Materials
Relating to the Measurement jof Priority Pollutants, Washington, DC,
June, 1977- [
^
24. Dry Color Manufacturers Association, Appendix E of the comments
made to the proposed rules on the "Manufacturing Processing,
134
-------
Distribution in Commerce, and Use Bans of Polychlorinated Bephenyls"
as appeared in the Federal Register on June 7, 1978.
25. Olofosson, John A., Paul L, Bishop, Dickson, Richard A.,,
"Physiochimical Treatment of Lithograph Wastewater". A paper
presented at the 33rd Annual Purdue, Industrial Waste Conference,
Purdue University, Indiana, May 9-11, 1978.
26. Raw Materials Index - Pigments and Solvents, National Paint and
Coatings Association, Washington, DC, 1975.
27. Raw Materials Index - Resins, National Paint and Coatings
Association, Washington, DC, 1972.
28. Raw Materials Index - Drying Oils, National Paint and Coatings
Association, Washington, DC, 1973.
135
-------
-------
SECTION XV
GLOSSARY
Additive
One of a number of materials added to ink in small amounts to alter
one or more of its properties. They include driers, antiskinning
agents, dispersing agents, waxes, lubricants, surface active agents,
etc.
Background Level
The amounts of toxic pollutants present in process intake waters
water) . :
BATEA • ' ' . ! •
(tap
Limitations for point sources which are based on the application of
the Best Available Technology Economically Achievable. These
limitations must be achieved by July 1, 1984.
Ball Mill . ' :-
A horizontally mounted cylindrical tank containing steel or ceramic
balls that reduce particle size of materials when the tank is rotated.
Batch
Any manufacturing or treatment process which accumulates a fixed
volume of material (i.e., wastewater) for processing, treatment or
discharge. Compare to Continuous.
Binder
The components in an ink film which hold the pigment to
surface.
Biochemical Oxygen Demand (BOD5) .
the printed
The amount of Oxygen required by microorganisms while stabilizing
decomposable organic matter under aerobic conditions. The level of
BODS is usually measured as the demand for oxygen over a standard
five-day period. Generally expressed as mg/1.
137
-------
BOD
Biochemical Oxygen Demand , !
[
Capital Costs j
Expenditures which result in the acquisition of, or the addition to,
capital or fixed assets. Costs associated with the installation of
such assets are included in capital costs.
by other
I j
Captive Manufacturing Site
A plant which only manufactures ink for internal use or use
divisions of a parent organization,
Carbon Black \
I
An intensely black, finely divided pigment obtained by burning natural
gas or oil with a restricted axr supply.
i
Caustic Rinse ,
—— i ^ _; ^
The cleaning of residue froih ink tubs with a caustic solution. See
Closed Loop Caustic System, Open Caustic System and Partial Recycle
Caustic System. !
Caustic Soda ; .
In its hydrated form it is called sodium hydroxide.
I ,
Chemical Oxygen Demand (COD) ;
A measure of the amount of organic matter which can be oxidized to
carbon dioxide and water by a \ strong oxidizing agent under acidic
conditions. Generally expressed as mg/1.
f '
Chemical Treatment •
A process involving the addition of chemicals to wastewater to induce
the settling of solid matter and remove dissolved materials. Materials
commonly used in chemical treatment include polyelectrolytes, lime and
alum. (See also physical-Chemical Treatment.)
Clarification ',
Any process or combination of (processes, the primary purpose_of which
is to reduce the concentration of suspended matter in a liquid.
138
-------
Closed "Loop Cans-tic System
A tank cleaning system which recycles a primary caustic rinse and uses
all of a secondary water rinse as make-up water for the caustic.
(Compare to open Caustic System and Partial Recycle Caustic System.)
COD
Chemical oxygen Demand
Continuous i
Any manufacturing process which produces a continuous flow of product
or wastewater and treats or discharges wastewater at the same rate at
which it is generated. (Compare to Batch.)
Contract Hauling ;
The collection of wastewater or sludge by a private disposal service,
scavenger, or purveyor in tank trucks or by other means for
transportation from the site.
Cost Center >
A business whose objective it is to accomplish its mission within cost
or expense parameters. A cost center realizes no income.
Discharge of Wastewater
The release of treated or untreated wastewater to a receiving water,
POTW, or any other location that is off-site. Examples of instances
where wastewater is generated I but not discharged are total recycling,
total on-site containment, contract hauling of wastewater, and total
evaporation. :
Disperser ! -' .
Mixing machine that acts to disperse the components-of ink.
Dispersing Agent ,
A reagent that is compatible With the solvent and holds finely divided
matter dispersed in the solvent.
Drier
# . .
A composition which accelerates the drying of printing ink or varnish.
Driers are available in both solid and liquid forms.
139.
-------
Drying Oil
An oil which readily takes oxygen from the air and changes to a
relatively hard, tough film by[oxidation and polymerization.
Epoxy Resins ;
Plastic or resinous materials used for strong, fast-setting adhesives,
as heat resistant coatings and:binders, etc.
Equalization
Any process for averaging variations in flow and/or composition of
wastewater so as to effect a more uniform discharge.
Evaporation of Wastewater . :
i '
A disposal method in which natural or induced heat causes evaporation
of wastewater.
Extender
See Filler. ' ;
Filler i j
Inert substance in a composition to increase the bulk, strength,
and/or lower the cost, etc. [
Flexographic Ink
Quick drying, low viscosity ink based on volatile solvents that are
used in the flexographic printing process. Flexographic inks can be
water-based. ;
Flotation
Dissolved Air Flotation (DAF) or dispersed air flotation, which are
processes that inject air into wastewater causing dissolved and
suspended material to float to\the surface for removal.
Flushing
A method of transferring pigments from dispersions in water to
dispersions in oil by displacement of the water by oil. The resulting
dispersions are known as flushed colorfe.
140
-------
of Was-tewa.-fc.er
The process whereby wastewater results from the manuf act taring process.
Wastewater may be generated but not discharged. (See Discharge of
Wastewater.)
Gravity Separation
Any process in which oil, grease, skins, or other floating solids are
allowed to rise to the surface, where they are skimmed off, while
heavier solids are allowed to ; settle out.
Gravure Ink
Quick drying, low viscosity inks based on volatile solvents.
Heat Se thinks . • ;
Letterpress and lithographic inks which dry under the action of heat
by evaporation of their high boiling solvent.
Ink ;
See Printing Ink.
Inks, Quick- Setting
These inks for letterpress and offset dry by either filtration,
coagulation, selective absorption or often a combination of these with
some of the other drying methods. The vehicles are generally special
resin-oil combinations which, after the ink has been printed, separate
into a solid material which 'remains on the surface as a dry film and
an oily material which penetrates rapidly into the stock. This rapid
separation gives the effect of very quick setting or drying.
Inorganic Pigments
A class of pigments used i,n printing ink manufacture consisting of
compounds of the various metals. Example: Chrome Yellow.
Lago-on ;
A shallow body of water, such as a pond or lake, which can be used for
impoundment for purposes of storage, treatment, or disposal,
141
-------
Landfill
A solid waste land disposal technique in which waste is placed in an
excavation and covered with[ earth. Wastewaters land sludges may
occasionally be disposed of in landfills.
Letterpress Ink ;
I
Ink used for typographic (raised type) printing which is a viscous,
tacky ink which cures by oxidation,
Lithographic Inks
Inks used in the lithographic process. The principal characteristic
of a good lithographic ink jis its ability to resist excessive
emulsification by a reservoir of dampering solution.
Metallic Inks i
Inks composed of aluminum or bronze powders in varnish to produce gold
or silver color effects.
Moisture-set Inks
Inks that dry or set principally by precipitation. The vehicle
consists of a water insoluble resin dissolved, in a hygroscopic
solvent. Drying occurs when the hygroscopic solvent has absorbed
sufficient moisture either from the atmosphere, substrate or external
application to precipitate the binder. An important characteristic of
these inks is their low odor. :
Mineral Spirits
A petroleum derivative used as a vehicle for inks and varnishes. It
usually boils in the range of 149 to 204°C (300 to 40b°F) and has a
flash point just about 27°C (1pO°F).
(
Mixing
The incorporation of ingredients into a coating with the use of little
or no shearing energy. '
NPDES (National Pollutant Discharge Elimination System) Permit
A permit issued by EPA or an| approved state program to point sources
which discharge to public waters allowing the discharge of wastewater
under certain stated conditions.
142
-------
Addition of acid or alkali until
(i.e., pH = 7) . ;
News Inks
the pH is approximately neutral
Printing inks designed -' to run on newsprint, consisting basically of
carbon black or colored pigments dispersed in mineral oil vehicles,
which dry by absorption. -Recent developments utilize emulsion,
oxidation, and heat set systems.
Noncontact Cooling Water
Water which is used for cooling purposes but which has no direct
contact with and is in no way contaminated by either the manufacturing
process or contaminated wastewaters. In the cooling process, however,
it may experience a change in temperature.
*F
OSHA . '
I -
The Occupational Safety and Health Act.
Organic Pigments
General classification of pigments which are manufactured from coal
tar and its derivatives. Compared with inorganic pigments as a class,
they are generally stronger an'd brighter. Example: Lithol Rubine.
Organosol j
A suspension of particles in an organic solvent, most usually made
with vinyl resins, solvents and plasticizers,
Opaque Ink
An _ink that does not allow the light to pass through it and has good
hiding power. It does not permit the paper or previous printing to
show through .
Open Caustic System
Any tank or tub cleaning system that does not reuse any part of a
secondary water rinse following caustic-washing.
Operating Costs
Expenses necessary for the maintenance and operation of capital
assets, including depreciation, interest, labor, materials, etc.
143
-------
The reciprocal logarithm of the hydrogen ion concentration in
wastewater expressed as a standard unit.
POTW (Publicly Owned Treatment Works)
Wastewater collection and treatment facilities owned and operated by a
public authority such as a municipality or county.
Partial Recycle Caustic System ;
i
A tank or tub cleaning operation which recycles a primary caustic
rinse and uses only a portion of secondary water rinse as make-up
water for the caustic. (Compare to Closed Loop Caustic System and
Open Caustic System.) i
Physical-Chemical
The method of treating wastewaters using combinations of the processes
of coagulation, flocculation, sedimentation, carbon adsorption,
electrodialysis or reverse psmosis. As used in this study, a
physical-chemical treatment system involves the addition of chemicals
to wastewater to induce the[ settling of solids ,and removal of
dissolved materials, followed by mixing and sedimentation.
Pigment
- - - • I
The colorant used to give printing inks the desired hue and color.
Plasticizer
A substance added to printing ink to impart flexibility.
Printing Ink
Any fluid or viscous composition of materials, used in printing,
impressing, stamping, or transferring on paper or paper-like
substances, wood, fabrics,> plastics, films or metals, by ^the
recognized mechanical reproductive processes employed in printing,
publishing and related services.
Process Wastewater
Any used water which results from or has had contact with the
manufacturing process, including any water for which there is_ a
reasonable possibility of cpritaniination from the ink manufacturing
process or from raw material-intermediate product-final product
storage, transportation, handling processing or cleaning. Examples of
144
-------
pxocess vrastewater include wastewater generated £>y -tub washing or
floor cleaning, etc. Cooling iWater, sanitary wastewater, storm water
and boiler blowdown are not considered process wastewater if they have
no contact with the process.
Profit Center
— ' •"•~——^——~ e '
I
A business or portion of ;a business whose objective it is to con-
tribute income over and above its expenditures and allocated charges.
Public Waters
All navigable waters of the United States and the tributaries thereof;
all interstate waters and tributaries thereof; and all intrastate
lakes, rivers, streams and tributaries thereof not privately owned.
Purveyor
See Contract Hauling. :
Reclaimed
Water or solvent which has bee|n treated and restored for use.
Recycle of Wastewater
The piping of wastewater, whether treated or not, from its points of
final collection to a prior process step.
Resin
A natural or synthetic material that is an ingredient of ink and which
binds the various other ingredients together. It also aids adhesion
to the surface. : ;
Reuse of Wastewater
The collection of either treated or untreated wastewater for the
purpose of utilization in a prior step of the manufacturing process.
Scavenger , ;
See Contract Hauling
Screening j
Samples taken of untreated wastewater only to determine the absence or
presence of toxic pollutants (see also Verification).
145
-------
Settlement Agreement
i , . .
An agreement between the National Resources Defense Council (NRDC) and
EPA remanding 21 industrial categories, one of which is paint and ink
manufacturing and printing, for review of BATEA, including a study of
toxic pollutant levels. ;
I «
Settling
The process of disposition of sjuspended matter carried by a liquid by
gravity. It is usually accomplished by reducing the velocity of the
liquid below the point at wh'ich it can transport the suspended
material. ;
Shellac
An alcohol-soluble natural resin widely used in flexographic inks.
Silk Screen Ink
-.....-I- jm«-m,nf-iT_«n. -— - ^
Quick drying, full bodied, volatile inks used in the silk, screen
printing process.
Skimming l
The removal of floating matter that has risen and remains on the
surface of wastewater. '
Sludge Conditioning
Treatment of liguid sludge by chemical addition, dewatering,
filtration, drying, or other methods.
Spray Irrigation
Transport of sludge or wastewatier to a distribution system from which
it is sprayed over an area 4f land. The liquid percolates into the
soil and/or evaporates. None of the sludge or wastewater runs off the
irrigated area. ;
Solvent-Ease Ink
Inks which use oil or solvent as the primary vehicle.
Thermosetting Ink
A thermosetting ink is one whiqh polymerizes to a permanently solid
and infusible state upon the application of heat.
146
-------
Solvents, diluents, low viscosity oils, and vehicles added to inks to
reduce their consistency or tack.
Tint - .
A very light color produced by adding a small amount of color to an
extender.
Total Organic Carbon (TOG)
-A measure of the amount of carbon in a sample'originating from organic
matter only. The test is run; by burning the sample and measuring the
carbon dioxide produced. ;
'- ' /
TOC
^ - - / I . ' " ' '
Total Organic Carbon i
Total Suspended Solids (TSS)
Solids that either float on the surface of, or are in suspension in,
water and which are largely removable by filtering or sedimentation.
Toxic Pollutant
/ ':
One of the elements or compounds on a list of 129 derived from the
Settlement Agreement (See Appendix E of this document).
Treatment , - ' >
Any process of conditioning water, wastewater, or sludge prior to use
reuse> or discharge.
Varnish , '
A transparent, liquid that . dries on exposure to air to give a
decorative and protective coating when applied as a thin film
Varnish may be made by reacting an oil and a resin at high temperature
and dissolving in a suitable element (Cooked Varnish), or by blending
a previously made resin with a solvent (Cold-Blended Varnish).
\ i . "
Verification .; '
A sampling program including samples of untreated and treated
wastewater and sludge to determine the levels of classical pollutant
and toxic pollutants known to be present, as well as removal
147
-------
efficiencies by various wastewater treatment processes. (See also
Screening.) !
Volatile Fraction ',
That portion of a ink which evaporates from the film Curing the drying
process.
Water-Base Ink
Inks containing a vehicle whose binder is water soluble or water
dispersible. ; !
148
-------
APPENDIX A
DATA COLLECTION PORTFOLIO
149
-------
-------
A.
1.
2.
S.
7.
mx ^ssaauazaa njousntir SURVEY
ganaral Information (Sotas For Multiple Plant Companiaa, Coaplata on*
questionnaire for each manufacturing aita.)
Naaa of Firn , " '
Plant Ideation and Mailing Address
(including zip coda) • ;
3. Telephone Number
4. Mama and Title at Respondent
S. .Address and Telephone Number at Saspondent (it different)
Indicate your type of .busine«a organization
-------
10 ladieae. th. nnmb*r of th. various si» Iload and jcrtabl. irJc =anufac=uri=g tubs (tanks) at your plant th»c
rtquSrelaania, (us. clos.st tab sis. shovn). Do not inelud. any d«iicat*d «or.a. tanks (i... solvent,
s«sin, «tc.) or Ball aills that ar. raraly or n«»»r el«ori«d.
Hmt>« of Ti^a
Mere th.in 50
?ch« Stz. (Gallons)
Lass n*"" 5
fr-10
10-50
51-100
101-250
asx-soo
501-1000
o»«r looo
11. Indicat. th. numb«r of
150-200 Q 201-250 [
^
G
G
G
G
G
G
n
G
days
H
i-3
G
G
D
G1'
G;
Qi
p*r y«ar th. ink
251-300 [""I
I
D
G
G
G
G
G
G
D
plane o{Mrat>s<
301-365 Q
G
G
G
G
G
G
G •
G
G
G
G'
G
G
G
D
G
G
C3
C3
G
D
G
G
G
12. indicte. th. a«r»o. daily wa«r con-nptica for ail us« ""(.*. cpiMtion 13) within th. ink manufacturing facility
(gallons p«r day)
0-10,000 Q 10,000-20.000 Q 20.000-30,000 Q 30.000-50,000 Q SO.OOO-WO.OOO Q Ov.r 100.000 Q
Actual (i£ known) 9Pd ,
13. Indicat. th. p«rc«vt of wat.r us«i for aacti of th. followingi
fareiint: of Total Mater O«a
-------
1. Indicate th* metnod(s) used to ciun ranks, tabs, filling machin*s, «te. (check as many as applicable) :
Water Rinse |~[ Caustic Hash Q Solvent Wash Q Dry Clean Op Techniques | | Periodic Caustic SoakQ
2.
Partial 8«cyela
If you us* a caustic system, indicate which tyo*:
Closed Loop (Conplet* Recycle) FJ ' Open (No Racycl*) j~~]
If you us* a water rins*, indicate th* water pressura ua*di
Less than 50 psi FJ 51-100 psi |~~| 101-150 psi FJ Greater than 150 psi[~""]
Indicate th* appropriate frequency for each of the following equipment cleaning or housek**ping operations:
All tte Tin* Hose o£ The Tin* Occasionally Mover
a '•; a p
;a
a
Clean tubs s*tu**n aaoh batch
itaus* apenc rins* uatar in
3ues*qu*nt batches
F*us* spent rins* watar to vwsh
tubs, aquipoont, ate*
a
a
G
G
G
b
G
5. Do you pick up spills using dry clean-up mthods?
S. Are any floor drains connected to th* itoia s*v*r?
7. Are any floor drains connected to th* sanitary sevoc?
G
G
G
G
8.
Indicate approximately how much water is used to claan ehe tab sizes listed:
7olun* of Mater naud ao Clean a Tanfc (gallons)
0-5
o--
n
a
a
a
a
a
6-10
a
a
n '
D
,a.
a
D
u-so
El
c
n
a
D'
' G
a
31-100
a
a
a
a
a
a
a
.-tore than 11
• D
a
a
a
. G
. G
a
9.
10.
If you us* solvent washing, is your spent solvent rodistilled? Yes I I So I I
Do you redistill solvent at this sit*? ; " ' Yes | | No h j
If yes, do you us* steaa injection distillation Yes [~"[ Ho F™]
If steao injection distillation is usod; what is tan disposition of th* contact staaa condansat*'
Discharged to stora sew*r | | Discharged to sanitary s*w*r [ | Mixed with cooling watar | |
Mixed with other process wastewatar f"l Oth*r I j '
11. If caustic is used for cub or equipment. cleaning, is spent caustic discharged to th* sanitary
3«w«r? Yes p| So j [ -, ..
12. If solvent is us*d for tub or equipment. cleaning, axa spent solvents discha'-.gad to the sanitary sever?
1.
Do you ua« v«t scrubbers in th« ink plant for air pollution control?
Which of the following other air pollution control dovicas do you utilis*? (Ink manufacturing operations only)
Afterburners j ] Electrostatic Precipitators [~~| Baghous* Collectors Q Cyclones j"^ Pilsars Qj
Other _
153
-------
3.
r.
Indicate which of eh* fallowing uastawatari aza eoabiaxi with tub cleaning vastawatsr bafore disposal;
««t Serobbar Q Boiler Slowdown Q Boiler Cleaning Q Hon-asntact Cooling Q Sanitary j~j Laboratory
A (indicate)
Wastevater Handling and Disposal
1. Total rolia» of ink process- vastavatar generated daily (gallons):
0 1-10O 101-250 251-5001 501-750 7S1-WOO Over 1000
Average
n a
0 G
G
G
G i
G :
G
D
G
G
G
2.
TnfMc-n»^ tha aethod(*) of ^<«r"wsl of wastawatar:
Caaplata tUfaf or Racycla I""] Evaporation I 1 | Partial Kcuse or Hacyele [""] Discharge of City S«w«r [j
^•aJ UneeT i Wesa* | |
Bave you Bade an application for an asnta p«rmit for process wastewatar? fa* | J "o | J
«av« you applied for and/or recaived an OTOES p«rait for csoling waster or stor»«ter runoff? Tas | J Mo | |
I£ yea to 4, 5 or 6 indicate tha nav* of stream or wmtar body receiving your vaatawatar
a. Ii proceu wai
aanicipalityi.
is discbarmd tr> dry i
the nazM and address of the sewar authority or
10.
u.
Indlcat* if tha ariicipality or j«xag« authority utiiiiaa any of eh« Jollowingi
lodiucriai Watta Ordinaoe* [~~|
S««»r 0«« CiargM or SurchargM |~~|
Uast«watae sanplln? at your plant | [
local p«rait zyitaa to discharge to tha siwar | |
Jl*qair«« you ts sazp;* and analyn your oira va«t»«at^r j [
I* your ittk pro=a«« vast«wat»r traat^ or conditional in any way b«for« disposal?
•D
M proc.«« wasewatar i* tr*at«l by th« plant prior Co aischarg.. iwUcata which wasts-mt«r strmams ar. scnbiawl
vita ch« procais vastas arior to ar.acaent. and t."* extant of sheir contriiution to th« waotwatar str«am.
Uajtewatar Source
of rotal Maatawater Strean Cndargoing rraacignt
01 1-20 21-40
Ink ?roces» Wastavatar Q Q | !
itaiin HaBofictoring I—I r~| I j
Uasuwatar I—I I—I I—1
SoUar Blovdown Q Q [""]
Air Pollution Control \] | ] [ |
Sanitary G G Q
Coaling Matar | j [~"j j |
Other G Q Q
11-40
D
G
G
G
G
G
G
€1-30
:G
G
• G
G
1 G
: G
i- n
31-99
G
G
G
G
- G
G
G
100
G
G
G
G
G
G
G
154
-------
12. Indicate Hathod<3) of wastewatar treatment or conditioning used at your sitai
neutralization
Settling or Clarification
Flotation
Chemical Treatment (polymer) | '|
Lagoon | J
Carbon Adsorption | |
13. Is your wastewatar treatment system batch ["""] ;
14. Is your wastewater discharge batch FH
| |
| j
Equalization I I
Evaporation ' | |
Chemical Treatment (lime) | i
Tritdcling Filter Q
Gravity Separation FH
Filtration; F"1 '
Chamioal Treatment (alum) [~1
Activaeed Sludge F~j
Chaaieal Traatnent (other)
or continuous | |
or continuous | |
15. Provide .the following information far your in-'plant wastawater treatment facility!
laar Installed 19__ ' | - '
_ Installed capital cost ($1 __ _ '
Approximate annual operating costs (S)_
Design volume
-------
2S. li you responded positively fas any of the analyse* listed above, please attach, data sheets jusmarizing the
analytical Information you have collected for the last four years. Indicate whether the analyses are Jor
uncreated or txeaeed wascewacer, and wnether rhe process wastevaear scream was combined with other waste ^
streams at the point of sampling.
26. Eatiaata the combined r.ev investment and total operating coses that will be required during the next Jour
years to aeec existing wacar pollution control regulations on tfa« local. 3ta.ce and Federal levels.
Total Maw Investment required S_
Annual Operating Costs i
27. Indicate which of the following miscellaneous regulatory areas you eacpecs.will require s^onificane investment
over thai next four years:
Odor [""I
Air PoUution Control
Therr-il,
(~]
Solid Waste j [
Sonic Substances Ace | |
Safe Drinking Water
IS. Estimate the anticipated new investawnc and aimual operating costs so aeee the carrent requirioents of these
other regulatory considerations over the next four years i
Total New Inrestaeac Required $_
Annual Operating Costs S
S. RAX ."ATSUALS •
Plus* eheck the. appropriate box for each clans of raw material which is used at this site (regardless of
quantity used) . If you are not positive abcuf the heading used, check the list of eradenames and numbers
and check the box if you use one of the materials listed. ., IS you use an unlisted material which is desc«i«d
exactly by the heading, checx the box? listing Che other material is optional* If there is no "other" listiid
for any category, checx the box only if one of the specific listed materials is used. Abbreviations used
for concany oaaes are listed at the end of this leceion.
DYES, FLCSHES. ANO
n
se LEAD
Cyascab Serie*
BaxBondi "anli-ii-h" Series
Eagle Picheri -S-P-202-, -E-P-303", -Z-P-»1"
Cacor* 4Sx
O«DE
Cheiecroni WT 6200 Series
Earshawt CR, JQl-TS
ML Ind.: Xequlsr (BtSJ r Red scar; Grade 101 FM-li
Oncer -23Ai 75RA> 7SRA2
Ctheri
I I zgg sciriaz PIOJSHTS
?era-0-U.th
Otheci
ASAJCOl -AZO--11.22,33,SS,S5LO,55Tr
ASAKCOt -AZCOOX" Series
£agle-?icher> "S-P-AAA, Series
M.J. Sine - "XX* Series
Otide* 30-P
St. Joe Minerals. *St«7oC" - 17, 20,40
Other American 71 no Oxidesi
n
ZIKC oxrpg
ASAKC3 - AZO 06, 77, 775
K.J. .Onct rior.nce Ore«n Seal - It -T&DOX' 2S.SJ.S
St. Jo* Hineralst *St. Joe* - 913.
Other:
I IgiTie yriiAi
-.B. DiTljl 50EW, 50SWJ, J134S, 533W, 533WJ, J13I.O
Ouponej r-539-O
Other:
^
COS? AND TUXES
M.J. Zinc: -Standard Zinc Oust" - 22,44,422, 444, 641
"Sigh ?uriiy Sine Ouss" - 122,222
•3.S. 3ron=e: 751, 752
Other:
D OTHER KCTAIilC fOWDEES AND rtSJCES a
XICXEI., SILVER. COPPES, LZan A
Alcan: *MD* Series
O.S. Sronie: "Cupro-Nickel"
Other:
D
Ferro Corp.: V-aa6O, V-8SSO, V-384O, V-3830, V-8S30
V-8820, 7-flS21, V-883S, V-H82S, V-834S
7-354O
General Color: 8OO, 80S, 313, 824, 827, 1000, 101
1020. 1024, 1027, 2000, 2012, 202C
2024, 2027, 301S, 3020, 3022, 3027
100S .
CUdden: •Cadaolith* 200 Serlest 2000 Serins
Harsh/no "Uthonnn* R«d" Serinsi C? 1401) Serlest
O> 1SOO Secies;
Hercules. X-2327. X-3327. X-2328. X-332II. X-2329
X-3329. X-2330. X-2947. X-29«S. X-2949'
: X-2950X
Other. Cadaiusi Reds:
r—I
RED. KAHOOX. CEtANGE
Cadmerc Series
Sarshaw: 18060. 18120. 18210. 18290. 1S370. 18410
C? Ofhirl'tn Series
Hercadiua Red Series
Other:
a<
*a. Cvanamid: "Sorwood Green* 10-3000 Series
Hercules: A-44OQ C.?. .Series
HYORATT3 CHUOMIDM OXTCE
n
Hercules: X-1010. X-1483. X-2944
Pfizer: GH-9869
C-ther:
n
CZRCKIOK OXIDE
F.3. Oavis: 3020, J 3310, J 53S1
Hercules: X-1134 C.P.. X-1861 C.7.
Pfizer: G 4099, G 5099, G 6099, 3 6139, G *099
Other
156
-------
• PIGMENTS, OYgS, ?tUSHES ASB OISPgaSIOHS. (Cant.)
D
CaDMUM YELLOW AMD ORAHGE'
Ferro: 7-9820, 7-9520, 7-9810, 7-9510, 7-8810, 7-881S
General Color: 920, 950, 970, €20, 640, 660
Cadmolith Serias ,
Glidden: 3050, 3150, 32SO, 3350. 3450, -3550 ;
Harshaw Chea.: 1400 Series; 1500 Series; Primrose - 20, 206,
23, 1400 Series,; Lemon 30, 306, 32, 33,
Yellow 4O, 406, 42, 43, 45, 456, Light
Orange 50
Hercules: X-2272, X-2273, X-2233, X-231S, X-2S21, X-2S2S,
X-2823, X-2824, X-232S, X-2326, X-3201, X-3203,
X-3205, X-2320, X-2326, X-294S, X-2946
Other Orlmi im Yellow and Oranges
I I CHROME
in. Cyanamid - fallow 40 Series, Primrose 40 1450, 1460
F.a. Davis - J1200 Series '
Dupon-f - I-758-Oi y-433-Oj 434 0, 469 D, Krolor KX Series
Harahaw: "Vallov 2000" Seriasi *Grallow" 39SO, 3951,
"Srisiroso" Sarias, Softax Series \ '
ffarcules: X-1937, X-3148, X-1945, X-2558, X-1899, X-2S48,
X-33S5, X-1S09, X-2541. X-33S6, X-2891, X-2774,
X-321S, X-2777, X-2778, X-321S, X-3480, X-1810
X-2035, X-3431, X-34S9 aanpart HR Med.
Oncotr W7.-A , ;
Hiefaea: 1561E. 1590, 1610E, 1610, 310SE, 310S, 8777E,
• 1678PO, 1677PO, 1605PD, 1640, 1670
Saichhold:. Yallow 45-100 Sarias, 45-200 Series
Other Chroae Yalloust :
n
canons
Harshaws 2201. 2204, 2213, 2205, 2209, 2203
Harmless x-819 CP Light
Other:
D
MOLYBOATS ORM1GE COtTIAIiliaa CHROMinK AHO/OR LEAD
Am. Cyanamid: Orange 400-8000 Series
Ouponts Holy. Orange-re Series; Krolor!: Or.Y. KC—789-O;
Krolor Or.?. KC-786-O; Krolor Red, Kr-980-^O
Barsnaw: "Ming,JJrange" Series
Hercules: Rex Orange Series, "Chili Red" x-3170,•
Rampart Or - X-3386, X-3390; Rampart ER Or X-3047
Hicham: Holy. Or. 1720, 1730, 1740 ,'
Reichhold: Orange 45-365, 45-366, 45-370, 45-382 !'i
Other Molybdace Oranges> . :
a
RED LEAD. LITHASGE. 3LOE LEAD, ETC. . ,
Eagle-Picher: E»gla 97 Redhead; Eagle 29 Lithargaj
Eagle 33 Litharge; Eagle Sublimed 31ue
Lead
Hammond: "Litaarge" 100X; Red Lead - 85%, 95%, 97% :
98%, Orange Mineral
NL Ind: • Red Lead 95t, 97%, 93%; "Fume* Litharge: ',
"Color Makers' Litharge '
Other:
a
PHLOXINE REP
I iLinttKESCSKT SIGMEtlTS COMTRIiHiC LSAD
HostasoiR 13-3397, 3398, 3399, U-5100
Other:
D
3LOS CONTAItmtS SILVER
Davis Co.: 4103, 448, 449, 4S8B, 41S6H, 45323
Xohnstamo: A4S7S, A9B29
Landers-Segal: S301F, 5303F, 5183P, 5400F
wittaker, Clark, Daniels: 500 Series
Other: ,-
D
D BROWN AMD GBlUf PIGMENTS CONTAINING ZINC
AND/OR CHROMIUM
Ferro: V-9U7, 7-9119, 7-9121, 7-5101, V-5102,
F-6109, F-S111, F-6112, F-«113, V-9128
Harshawt 7733. 7739, 7751, 7760, 7776,
Hercules: 10393, 10352, 10369, 10392, 10327, 10391, '
10378, 10328, 10363, 10394 . /
Other Browns and Grays Containing Zinc And/Or Chromium
D
BICE
Am. Cyanamid: "Cyan* 55-3000 Series
Hostaperm 15-1000 Series
BASF: "Paliofast" Blua - 6000 Series, 700O Series,
Chemtront BT-4510, 3L-4S21, 3T-4559, BT-4561,
BI-4S64, BT-4614, BT-4651
; Irgazin -Blue 3GT •
Irgalita Blua LGCD
Oupont: Monstral Slue ST Series, BL Series,
"Ramapo" Blue - 3P Series
Harmon Colors: 3-4714, 3-4769, 3-4773, 3-4804
Harshaw: "Zulu" Blua 4800 Series,
Hercules: X-292S, X-3374, X-3048, X-2303, X-3414,
X-3223, X-2371, X-2810, X-3367, X-3453,
X-26S8, X-2372, X-3241, A-4434,^-348S,
X-3527. X-912O. X-92!fl. MoB»Tft?h™ Bin..
Hilton-Davis:
-3527, x-9120,
30-0286, 30-0291, 30-0344;
SOF-R-CONC* 6-68-C-301
Konnstamt A5712 "Monafaae* Blue
Nicheaii "Shthalo" Blue 500O Series, U40>
Sandozi -Graphthal" Blue SNK
Son Chrait Sunf asc Blua and Peach Blua Sorian
Other Phchalocyanine Blues
Series
D
PHTHSLOCfaHIHg G8ESH
Am. Cyanamid: Cyan Gr'een Y1S-304O; 315-3100
Hostapera 1&-2000 series
BASF: Paliofast Green 3600, 868O, 3720, 9140, 936O
Cheatron: • GI 4SOQ Series
Dupont: Monstral' Green GT Series
' "Ramapo" Green B, GT-501-O
Harmon Colors>'~'a-5000 Sarias,
Harshawi "Zulu* Green - 3800 Series
Herculesi X-3166, X-3167, A-4433, A-4436
Hilton-Oavis: '30-031S, 30-325; SOT-R-CONC
6-€8-C-401 B.S.
!Cohnstama> a 1581, A 5776
Hicham: Phthalo Green 4000 Serias
Sandoz: "Sandorln" Green 3GLS
Sun Chaasi Sunfast Green 264-0000 Series; Sunrast
Serias; "Emerald vista" Green 264-444
Other Phthalocyanine Greenst
I 1 CORRO3IOH mHIBITING PIGMEtTCS COHTaiMIKC CHROMIUM
?.a. Davis: Strontium Chromate J-1365
Calciua Chromate J-1376
X-2865, x-2974 strontium Chromate
464
u..Harcules
Other:
a
CORROSIOH INHI3ITO1G PIGMEMTS COHTAISING ZINC
F3. Davis: Zinc Holybdate 0830, Zinc Phosphate 0852
"HALOX" ZX-lll.
HL'Ind.: Halzin SC-1, "Holy-white" 101. 212
Other:
I _ JcORSOSIOK nngBITISS PIGMEtlTS COtlTMaiKG LEAD
Sagla Picher: "Permox" 1-4-3, Ternox" X
Hamnond: P-7, c-9
Other:
IHOH BLUE CCHTAIMIilS CfAMIPES
JDIARILID2 ORANGE TONER (PICH1OROBENZIDEME-OERIVED)
An. Cyanamid: 50-0000 Series, "AUealoric", "Mile
"Blacxstone"
F.3. Davis: "Milori" Slue 4049, 4215
Harahawi "Hilori" Blue AR 4028, 4050
Sercules: X-640 C.P., X-2274 C.P., X-3163 C.P.,
. X-2235-C.P., X-1835-C.P., X-712 C.P.
A-984 C.P., X-3434, X-3340
Other: '' - '
An. c/anamidi "Oiarylide Or; "45-285O, "45-2880 Series
Aa. Hoechst: '5era. Or." 12-1000 Series
Chemtron: OT-5661
Harmon: OP-S833-
Herculea: X-2065, X-3082
Sandoz: 3272-0
Sun Cheat 276-2384
Other Oiarylide Orange Toners (Dichlorobenzidene Derived) :
-------
PIGKEHTS. DYSS, FLESHES ANO OISPERSICHS (cone.)
A». Cyanamldi 45-2555, 45-2650
A«. 8e«CJl»ei 11-1101, 1103, 1006, 1003, 1200, 1300, U16,
1300, 1216, 1012. 1013, 1305, 1125 ',
1012, 1013, 1305, U7*i
CIWKZOIU tT-8073, YS-8047, YT-6093
t* T«llow L3AM
Color*! V3-570O Sariu
Y«llow 1200 S«ri«»
Buculut 1-2435, X-1940, X-2476, X-2600. X-2382, X-338S,
X-2S38, X-2864, X-3446, X-3S3S, X-9340 |
Silton-0*»£»« Di-irrlid* r*l 30-0535j Sup-R-Csne 5«rins
XebnsUBU A9145, A9744. 33503, 13577, 13615
Hiebuu *»uuzidla« Y«l" 3000 S«ri«»
Sindoti 4233-0, 4335-0, 4534-0) 'Sriphtol YcllaV Kdi
Sun Cunt -Kac?30a Yd- 273-OOOO S«ri«i -TUdiant Y«l'
274-0000 S«rl««i -twoon Metallic- - 275-0003,
275-51291 "Siuylld* Y«l« 27S-O049> •Tranifara
ITSR- 275-2233 '
Otiuf Olazylld* r«llov Tonars (Dichlorob«nzid»n« D«riv*d) >
SLACK ?IG>i£tfa CC
I I
asns XKD MABCOHS (DicgLoscBgtarpEita
SiMchac: 13-1000 -Vcra R»d- VB
Calozai a-6200 SarlM
Stxxhxwi -IVrualixm 8*d* 1153
Sun OMI 'Aoiiea R*d- 236-5025
Othut
I— I tUSCZUAKZOaS REDS, MAROONS TCNZRS AMD IJUETS
I IcoHixtapc zmc, CHUOMTOM. ANO/CR
A*. So*ciuic> 13-4305 *?«za fink* E-O
OMttrom KT-53101 RT-5340I RT-539O
Ochxci
D
tastntjm.rras YEUOU AMD ORAMCE TCNZKS AND
ANTIMONY AHD/OR CHBOMIOM
BASTi Tulioail tallow*- -1690, 1770, 2330)
tMOioMt "!4«c»or Suii" 7370, 7376
•itauor Oring.- 7383
•M«t«oc tin* 7729
Oeit*z>
a
AMD ORANGE TOKERS AND
LAJXS coMTArtrnc COPPER AKD/OR
SASTl Tallotol I.llou
H«T-«h»vi
Othurt
1070
2912
(— l KISCZtiAHSOTS YSIXOU AMD GRANGE TOHEHS AMD LAKES r
I I CCiflXtNUC HIOSI.
SACTl TaliotOl Yallow* C830 >
OuPonei "Cr««a Sold' Y^-714-o, YT-562-D
Banhavi *Sun-Y>llov-S', NS310, C3320. •Son-auff ;
S33O
i X-3247 •r=vr«a» Grain Yalloir", 10401
n
_
sure, PURPLE AKS VIOLET
CTBOMICM
Terra i V-5200 31u*j V-5272 Blaa-CrMn, V-5274
M«d. Slu*
gii-ih»«i *X«t»ar Cetaklc* - BLa-7536
•itaMor Cabale* - BL 7550. 7556
*»«c«or Turquois«-Cob«lf "579
Oth*ri
I - 1 (USaQiMttOCS SLOE. POUPLE AND VIOLET PIGMESIS
1 _ I COKTXiaiHS CAOMICM
B«rcul««i 10312 *C*ral**n Blu«'
Cthmrr
D
Miser'r,Anreqs BLAO: ?IOGSTS eonrxiNiMg COPPER
r.rrot V-302, V-717, r-2302, f-6331,
Krxhawi .7S90 *!Ue«or Bk*
?«rroi -v-6730
Uurcului 10335 Hack
Ctiar:
a
XISCZLLANECCS YELLCW FIGMENTS CCHTAINISS
AMTIMCKY. LSAO. AND/CR
H«rcul««j 10315 Lwon fallow, 10324 Antxr,
10401 Yellow
Otbar:
D
sispmsiots - vrnirg'
,\urup«r3« Anriaonr Oxide M-320 ' XR LT3
Othor:
D
AQCE30S DISPCESICHS - SCO
Podvllz Vf-5031
Oeharz
tad*
(— lAQOTOOS OlSTERSICftS - YTXLOM (DIQCLORCBCalDENZ
I I
Colanyl Yellow OT 11-11O9
Aurup«r>« W-1041
Barcului X-2413, X-2453, X-3611
Saadoz: "Graptieol Yallov* 4534-2
Podall: W-3827
Otlmr:
a
KZSCZIIAKBODS
COPPER CH CSBOMICM
?erro. F 5686, 5637, 7637, 7610, 11633, 11649,
11655, 11656
Hinhtwi Sun 5r««n I. 9420, M«toor 741(i, 7459
B«rculM> 10342, 10329, 10307, 10402
Othari
I IAQOSOCS OISPESSIOKS - YTLLOK COBtAISISG LEAD
I IAKD/OR CHROMIUM
Hydrotin«R 0 .512, 0536
Aurup«r3e w-1031
Harahaw B-1133
Inaone: 991 3O22 CJiroaa Loon Ydllow, 991 038
ClrcoM H«diun Yellow
Podtll: H3013, W3S07, IH3499, W39O3. H3904
Aquaspcrsa 377-OOO-2065
ColortreiKl CP886S O
0£har Aqueoux Disparalonja - Yallow Cc:
and/or Chrooduats
I
nAQUEOOS DISJERSIONS - YELSCW COKBUHDC
AMD/OR CADMIUM
AurMp«n«R H1061, W1068
Hercul**i X-3291
Podall: W3941, H3946
Oth«ri
{ _ I
orspsasiCHS. - ORANSZ
Dtni«lt
20—59 >»lyb
-------
gIGMEMTS. DYES. FEOSHES ASO OISPggSIOKS '(Cone.
I 1 AQUEOUS OISPERSIONS - GREEN CONTAINIM3 COPPER i
I 1 AND/OR CYANIDES
ColanylR Green 16-2O05, 16-2001, 16-2010
Chematron: WDG-55, ' :
Daniel: BD2744,. UL20-77, OCS 10-70D, AC 66-78, OL 20-79
Hydrotint D-3658
Aurasperse M-60U j
"Aquis" Manastral Green - B.GW-749-P >
Harshau: "Thalo" Grean MC-O
Imparsa' Graan - X-2346, X-24S4, X-2689, X-3244, X-3288,
Hilton-Davis: 6-11-B-462: 6-ll-B-432» 6-33-T-410 '
Inmont: 991-8-O41 "Phthalo" Groan a/Si 991-006 "Graan
Phthaio" Y/A ,
Landers-Segal: 3336D "Phthaio" Graen w.o.
Podell: W-26O3A, IW-2829
Sandoz: Graphtal Graan 5869-2
Aquasperse 877-000-5 SU
Cal-Tint HC-3022, 3046, 3011 ' '
Colortrend GP-8811D !
Tennecb: "Thalo" Grean 897-000-5501 :
Other Aqueous Dispersions - Grean containing Copper
and/or Cyanides: , ;
I I AQUEOUS OISPERSIONS - GREEN CONTAINIHS CHROMIUM
Danial: gcs 10-72K !
Hydrotint D-310
Aurasperse W 6O17 . ;
Harshawr Oxrooiua Oxide HC-K
IMPerse Green X2722, X3289 ,
Podelli H-203S, M2607At. W2817 1
AquaSpersa 877-000-4205
Cal-Tint OC-30OS • • ' '
Colortrend GP-8805K . :
Other Aqueous Dispersions - Graan Containing Chroisiuas
| 1 AQUEOUS DISPESSIONS'- S1OE COWtAINISG COPPES Z8O/OS.
I ICYAMIDES !
ColanyAlue 15-1006 i
Chemetroa HDBS6 >
Microsol arillianc Blue 4G Pasta ~
Oaniai: AC 66-27, WD 2223, Ol 20-26, OCS.10-20E
Hydrotine 04S46
"Aquig" Monastrai^w-37z-t, HW-431-P )
Auraaparse W4123 ]
Barsnawj "Phthalo!1 Blue MC-E, 3-4011
IMPersa Blue X-2345, X-2446, X-2687, X-2688, X-2663, X-3221
X-3496 ',
Hilton-Davisi 6-11-3-32S "Shthalo" Bluet 6-33-T-31S "Phthalo"
Blue (S.S.I . ;
Inmont: .991 037, 991S-O4O;.
Kodis Blue ti-21
Podell: W-6402, W-6307R, 1H-62934, IW-«942
Sandozs "Graphtol" Blue 6812-2, 6325-2
Tennecoi 8|5-OOO-7202'"Thalo" Blue '
Aqua-Sparse "THaio" aiua - 377-OOO;7026, 377-000-7214
Cal-Tint' alua ac-3O14t Colortrand Blue - G? 8814E '
Other Aqueous Dispersions tBlue Containing Copper And/or cyanide
I [ NOB-AQUEOUS DISPERSIONS - RED CONTAINING
I I eapMitm AMD SSIBIIDM
Inmont: C|daiium Red - 5419, 5420
Chroma-Cal Cadmium Had 850-000-0601, 350-000-0301
Other:
D
NON-AQOZOCS DISPERSIONS - YELLOW CONTSIBING
LEAD AND/OR CHROMHIM ,
Daniel: Chroma Yellow - At 405, AL 409
Alkytint Chrome Yellow - S-536, S-5507
Hilton-Davis i Chrome Yellow— S-24-A-200;
S-24-A-203; S-24-A-206> 5-42-A-201j
- S-42-A7206i 5-83-P-3S3f 5-21-9-212
Auraeota Chrome Yellow 5-SO-?-36S '
Inmont: Qirone Yellow 3,6i Medium Chrome Yellow
2347, 2612, 4904, 5413, 5414, 6258
Oni-Cal _-66 - 6604M, 6665X
Chroma-Cal - 350-000-2006
Tennaco: Chrome Yallow - GSD 2006: GPO 2510
Other:
i - 1 NON-AQUEOUS DISPERSIONS - YELLOW '
I I (BICHU1ROBEMZIDSNE
Inmont: Diarylida Yellow 1178, Transparent Yallow 1198
Other:
| - 1 NON-AQUEOUS DISPERSIONS - ORANGE CONTAIHIHG
I _ 1 LEAD AND/OR CHROMIUM
Oaniai: Molybdate Orange: AL SIS, UL 2069
_Hilton-Oavi3 : Chrome Oranga S-24-A-60Ot Orange
Bland S-24-A-609; Molybdata Oranga
5-24-A-616, 5-42-A-«12j 5-83-P-635,
, S-42-A-61S, S-21-P-603 -• •
Auraeote Holybdata Orange 5-50-R-639
Inmont: Molybdata Orange 840, 2377, 4905, 5415, 6264
Tanneco: Moly Orange GPO 0940
Chroaa-Cal 850-000-O903
Other:
D
NON-AQUEOUS DISPERSIONS - BLDS COMTAIMiaS LEAD
AND/OR CHROMIUM
Chetatroni
Other:
"SCOT" fS-89Si "SCOT" RS-957j "NCMf- HS-1197J
"BCOT" RS-1795
D
AQUEOUS DISPERSIONS - 3UJE CONTAINING SILVER
Hydrotint D4053.
Kodis Blue AD-23
Landers-Segal: 5494-0 Ultramarine Blua,,WD
Podall: W-6032, IW-6940
Aquasperse 317-000-7504 Ultra Blue '.
Cal-Tint' Blue - UC-3074
Other:
D
NON-AOUEOOS. OISPERSIONS - BLUE COHTMNIHC SILVER
Alkytint 5448
Danial: AL 221
Inmont: 6297
Tanneco: 7504
Other:
r-1
! ; NON-AQUEOUS OISPERSIONS - USD CONTAINING LEAD
Red
Daniel: AL625
AlJcytint' S-5022 Le. Molybdate Orange
Hilton-Davis:
other:
'Quinacridone"
! Lt. Molybdat
5-42-A-123 Toluidine Rad, Dark
| 1 NON-AC.UEOUS DISPERSIONS - GREEN CONTAINING LEAD
• I | AND/OR CHROMIUM •
AUeytineR Green S-310
Danial DCS 10-72S
Tennecoi GPO-4Z02O?, GSO-4509 CP, GPO-4208, GPD-5103'
Hni-Cal 66-6605
Other:
l: I [NONiAQUEOUS DISPERSIONS - GREEN CONTAINING
I [COPPER AMD/OR CYANIDES
Hostaprint Green 16-2008
Chametron: "Phtftalo" Green FS-7S4> FS-958:
- FS-1192, FS 1794
HicroLtth Green G-A, G-T, G-K ;-
AJJcytint Green S-317
Daniel: "Phthalo" Green - AL 703, UL 20-77,
UCS 10-70D, AC 66-78, OT 75-74, EP 30-7t,
ST 47SO, AL 745, UL 20-79,
Hilton-Davis: "Phthalo" 3reen - 5-24-A-400,
S-24-A-40S, S-42-A-4O7, 5-42-A-411, 5-24-A-435
S-83-P-401, S-42-A-400, S-33-P-401, S-21-P-441,
5-21-P-444, Chrome Gr. 5-24-A-406
Auraeote . Phehalo 5-65-A-427 -
•Innbnt: Chrome Graen 1, 809? "Phthalo" Green
1083, 1168, 1199, 1245, 2330,'2610, 3035,
5412, 5447, 54r2 '
Podeil: 2000 Sariea prafix AL. AH, AME, AV, c, CS, CU,
DU, LA, LC, S, VT, Y
Tennacoj CTD-5503, GPO-4S03-L?, -AD-5503
Uni-Cal 56 - oollR
Chroma-Cal" Green 850-000-3001
Other Non-Aqueous Dispersions - Green Containing
Copper and/or Cyanides:
159
-------
ores, nesses XBD 3is?sasion3 (Con-e.)
(— I SOM-AQCE003 OIS5ERSION - 3LOE COHTAINIJC COPPER.
I J AN3/CR CfAMISES _ ^_
I l
OteP-saSICHS - !3UE CCNTMMIia SILVER
A3R-K
Alkytint 54213, 54SS7, S-1B2
S*ni«ll At 201A. AL 231A, AL 29€B. AC 66-27, UT 7S-28,
CT 30-23, it 4260, ML 297R, AL 298, UL 20-26.
UC3 10-20E
Biltoa-C«vi»«, "Cxin««» Blu«" 5-24-A-304, 302i 'ghfhala
Blu* - S-24-A-306. 304, 308, 309, 311.
5-21-P-33S, 337, 5-4Z-A-312. 305, |
S-S3-P-300.301
Auracot« Slu« S-45-A-39S
1190. 1202, 1211, 2609, 5444, 547S, 3034,;
4914, 1077, 4916, 9024, 2327, 5498, 6150,
6000 S«ri«» prefix At, AX, AKE, XV, C, CS, DO,
tc. s, SR, sr, VT. *
CTO-7309. 7209,
Oni-Cal £6_- 6608P, 6614O
Cnra*»-C»l - 150-000-7202
Othur Bon-Ao»ylie
Acidi Oi««arl E»t«) Ethyl ?oraie Eit«r: Phtha.lic Acidi
Diathyl E»t«rs Ethyl M«th»no»t«i Eehyl Phtiv«lJ.t«» Foroi
EChari •Snorol", "Ar«<7in«l" , TV««nttin«"; "Psl*tinol A";
•Plreaalol"; "51»cidol«"; "Solvanol"
Otimr:
I I PLASTICTISBS cotrnmaiic DI-Z-STHYLHEXYI,
OOP, Phth»lic Acid, Oi-S«c-Octyl-Phth«Jl*e«
Jcyiluc DO?
o-DOP
OOP, PX 138
Suticizu 215
Othur
'DJ
Ochurt
L:c SOAPS ASP
s ;cs?rrs CCNTMKTMC a
A*ro Mo. 4S O.S.P.i Dliaond 'Zinc St. H", 'ilnc St. OSP',
•Zinc Se. OS^ 603", "Sine St. 639C"; Nuodax US?, ;01G-10, DtS-20,
T«chnie«l» Plynoath XXX-B. SI-36, SI-50, So. 21: i
Uitco TUKjaiaXf L» V12S!S,
V133i V1S77, V134I 71298, V152: V1399 . V1026!
VT.420, V1048t V1S03, V1204r V1SS5, V1216; Vl'572
Otiar Stabilizers Containing Zine and/or Cidaim:
1212A. 1776,
2020: 5444
5330, 6V6A
-10-
160
-------
CHEMICAL SPSCJAtTlES (Cent.)
n
STABILIZERS CONTAINING LEAD OS. PHENOL
Intaratab W-24
Troykydr Anti-Skin Special Mod.
Anti-Skin Odorless
Other:
I I WJ.TJNO AGENTS CONTfllimia PHEKOL
Sianond: "Hyonic" Series
Witco 936, 960, 930
Other:
n
MISCELLANEOUS HETTINS AGENTS
Aerosol;: OS
Troyaan Zinc 3 , ,
i—1 VISCOSITY SUSPENSION S FLOW CONTSOL AGENTS
I [CONTAINING TOLUENE .
Pliolitaa AC-3 • .
Other:
AHTI-SlCTHNIiK! AGENTS COMTaiHIMG PHENOLS
n
"Cuaiacol SpeciaLC"; Troykyd" Antiakin Special
Modified, IBoyteyd AntisJcin Cdorlass Liquid.
troykyn Antisfcin Si Sevillac 10, TS
Other: \
n
PPESSSVATIVgS
"Intercida"'PMO 11*, PMA 1S», SO
Huodex PMR-18, PMO-10
"Troyaan" CMP Acataca. PHA10 SEP, CMP 10 SEP, PMO 30,
. PUB, Mercuric Oxide, PMA 30, PMA 100
•Super AO-lt"
Other Preservatives Containing Mercury
n.
CONTAINING COPPER
Intentab "Capper Naphthenata" 6%, 3%
"Tntercide" copper 10*
Insotral" CQ-A. CQ-WR, CN8
"Nap-All" Copper Naphthanate
"TJvaraoJj" Copper Haphthenata
Troysan' Copper 3
Hitco" Copper Naphthenate
Muodex Copper Naphthenata
"Quindex"
Other Preservatives Containing Copper:
D<
CONTAINING PSNTACHLOROPHESOL (PCP)
Oowicide S, EC-7
"Santobrite"
"Penta"
"Santophen-20"
•5CP"
Other PCP Presermcivea
n
"Interatab" Zinc Naphthenata 3%
"Ttoysan" Zinc 3
"Vancida" S1Z
."Bap-All" Zinc Naphthenata
"Uverrol" ^^^** Naphthenata1
Uitco Zinc Kaphthenate
Other Zinc Preservativaet
n
OTHER PRESEBOTITIVES
Dovacide A
I - 1 OSXIHC Oil. MOOtE-IED AUCCD SOLUBLE
I _ ISAPHTHALSNB _ .
OR COHTMfTCNG
Aroplaz 310-V-SOj "Coroc" L-26-34, S-47-H4, S-4700-a4j
Reliance AL-4313-HA-50, AL-3617-SA-SO, AL-4409-HX-SO ,
.AL-4313-HA-SO, . ;
Other: ;
r— I OICOSG on. MOorrtEo ALKIO SOLUBLE ra OR CONTRINING
I I TOLUENE OR ^'X '
Xoppers: 1330-27, 7365-SS-70
Haliances AL 4310-T-50, AL 4323-T-6O
"Synraaatar D-30360-T, W-7170-T
Other:
n
NOH-ORXIS5 i SEMI OXIDIZING OIL MOOIFIZO ALXZO SOLOBLE
Dl OR CCNTAIIgHG SZSXZBENZEltS OR TOLOENB '
Concheoce 323-O10 ' f
Xoppers 99-4, 99-ES-70; -Mirasol" 123-6-T, '131. 902, !
RCI-12-O10, 12-021; Helianca AL-2107-TX-60 , AL-2313-TIB-SO,
AL-4106-1S-75, AL-4129-T-60 ; ^Synraaata" W-7170-T '<
Other: " I "
| - 1 RESIN MODIFIED AUCfDS SOLUBLE HI OR CONTAINIMG TOLUENE
' I OR H
Aroplaz 1031-T-70: "Mirasol", 214 , 202-A> Rd 10-O10, ,
Reliance AL-3321-HA-50 Varicyd 310-SOHS
Other: ' '
I - ICOPOLXMER ALODS SOLUBLE' IS OR COSTRISIK3 TOLUENE OR
I _ I NAPHTHALENE _ I
"Chempol" !3-2444i "Synresata" O-98SO-S, TP-134-OAi |
Reliance SY-2003-VT-SO; "Salpol" 3713-'50E ' '
Other:
(— [CSL1OLOSE RESINS SOLUBLE IN OR CONTAINING MET3TL
LJ CHLORIDE OR TOLUEHE _ ___________ •
Eastnan "CA" Series, CAB 381-O.I, CAB 331-0. S,
CAB 331- 2O, CAB 451-1. CAP 432-0. S ;
Other: , '
n
POLXESTER AUSmS SOLUBLE IK OR COHTAINING TOLtTHNE OR
MftPHTHALZMS
Aroplaz 6022-S-6S, 602S-S-70, 6029-S-<5Oj Capjill
6619/6619-70, 6620/6620-60t "Synreaate" W83270EX03,
H876OS
Other: / .
I IEPOXX SOLUTIONS SOLUBLE in OR CONTAINING
"EPI-REZ" - 2047; Armldite* S71-T-7S, 597-ST-5S,
.597-EX-S5, 597-ST-SSj Dow D.E.R. 671-T7S; GanEpoxy
526T-25, Epotuf^ 33-S08, 33-507, 33-519
Epon Resin 1001 ST 70, 1001 CS-7S, 1001 FT-7S, 1O01 T-7S
10O7-CT-55, 10O7-KT-SS> Vanoxy 201-T-7S, 2O1-8T-70,
201-FT-7S, 207-iW-SS, 207-CT-5S
Other Epoxy Solutions Soluble in or Containing Toluene t
I IPOLXAMIDES SOLUBLE IN OR CCNTAININC TOIJENE
'CI3A Polyanide" 800IT60, 81ST-70; •CropoliOid" L-100 IT;
Saery "anerez- 1SOO; Varaamid 400, Epo'tuf 37-621. 37-648,
'anAnid 3rtrt «"--=rt
%her:
D™ '
UREA
VanAnid 30O ET-60
Other:
bt ca coNraiiiiac TOLUEME
Reliance AM-1008-IT-SS, AM-1012-IT-5S
Other:
a
RESINS soLnaLS is OR GOHTAimas MAPHTHRLSNE
Mnlnar 243-3
Other:
n
VIHK, SOLIDS. PVD (SYBTHESIZED ?ROM VINYL. CHLSRID'Ei
APCI "PVC" Series; Goodsuar "Pliovic" Series i
OCC - Trap: VYNC. VYBD: QYUtf, VTLF; CVK7, VTSS; '7ITV,
VYNWi QYJV, VAGH; QYOH, VAGD; QYSL, VMCH; QVSJ,
VHCC; S-2000; VMCA; VXDS, '^ROH; VTCDS-66, VERR;
"Saran aesin" ?310
Other vinyl Solids, PVC:
161
-------
r"l>oiaviH«, Msan isYirrgESizsp raoM vran. CHLORICE), M s-mugre a vrrei, roicsre SOISHLS :n -rpta
:* »7, ais, i2S. 1100, saoo, Asasis
f— IJOX3VD1H. AtCOBOt, FORMAL £ SO«SM. SOlDBtS HI
[ _ jog cetrtAiHias PKEMOI. OR TO
Sului occ XXSL. rrss. EMC, EDBH
t vpntLSjga
Other:
D
S«ria»f "Saxan tacax- 143» folidaaa S«ria»
s
S01I33 SOUBLg IX OR CCTTAINIMC TOS
Acryloid'" I«8U, 350, B66. 267, S72. 382
I J
re soumcMS scrsatr IM on cstmnrcc i
311—tQS,- 311-1301 O.v»cit«a 6011, 6012, 6013.
8014. 6016, 60241 G Car. 867 RJ» 60, 868 RHF 6O,
*69 KBT SOr Acryloiir fc-21, A-21LV, i-44. S-48S,
»-50. B-66, 8-72, B-82. S-fl«. »-99, C-lOtV
Oth«ri
soumix a o*
«i««
lurlonr S«i«« ;
Othmri
I IpBaMLie assiss
>xof«n«R S«ri««j Aa2j«rolR STS137, Sup«r Secitacitm '
S«ri««i Raiehold (V) 29-000, 100, 4OO S«ri««:
DCS CK-12B2, CK-1634»
3EJ.-JS20, SKS-2315, SX5C-245S. BKS-2600, BtS-2700,
1KS-2750I Aa«rOl ST-149f OCC "CS" S«riu, CKSS-2001!
7«ntalyn
*sh*BC3*
oehwr ;h*nolic
.^R
p-i OLSORESISODS VRBNXSSES SOtSBlX IS OR CCSTMSIW
I _ iPHENOT, Ca STHYtaUCSHS '. __ ] _ , _
Con=h«aco 385-0031 Tenneco 2-12B; KeCl:»X«y
12225-54 SSD, 10424-55B, U233-SSEND., H32S-SO ESB,
735-41E, 10917-54EKD, 1633-58E, 162S-60N! Syncon C3-3-SO,
3024-65ENO, 133S-56E, UlSOrSlND. 10731-461, 10931-28E,
2211-46E, 320-50na3i Xalvnr' G-«3a-<06, G-S81-50H
Chempol 15-2509, 15-2518; Mjucvar 2Slfi, 2S98> Syiicon"
S«ci«a, ?-24'7, r-121.. 'losa, HIS.,
"L*vrcnr" SEries i "Sop«rior" S«r±e« ,
Oth«r Oleorulnsus v»miiii«« Solublo la ac
or -
nsiii
HapH
soLoats is OR cosraisiJjs wiana oil
OCC-R-12J Carqill 6106-60
Ocbor:
I IMKLEIC sarsnciis sormrs m on CONTMSIHS T
ArociiMR S20T: syncon HAS6OT
a a earamae
78-|OT, Sjwncer XP 1857i "Synre»«i:«' a83270
EX03> Sp«nli£« Wl-301j Sp«no«r 3V -MOO" S«ri««
Otbwr:
[—I M1SCILLANEOCS SOU/BLS IM OR CCHTTiUIIUS T
I I KETgYI. CEZ^RIEg. OR TSICHLCP^gTHYt^yE
ElvaxR 40 i "Visas' PE207, PI2071T, ?E222, PT222T, PS307,
PE3077, VPESS45A, VPE S571A..J HCS 10-V14
Ochar:
CipuolR a»nz«r«j B«oi«r.« (Nitrttion Grid.) I
"3«niol", •Cycloh«x«tri«n«" Co»l ttaphtiia. Benzol Sydcids,
Othur: ^
LJ B
?Ot3BTE MIX
SolVX, "Solv1 A-3Q, 'Sol*' \-el. "Solv1 A-lOOi
Cyolo»ol 27", 2»l EsjiMOl 7200-\l Slc«ily SK-69 [
Oth«s:
I l-
Sip««olR 1° Tolu«n«, 7200, ticcol Spirits
Toluolj H«thyl-3«ni«n«.- M«etaeid« ?henyln«eh«n«i Toluonol
Oe^crt
I i
AKICO Sol» 3» Oyelo«ol 37
tap«»oi Sthylbanr«n«» Asuco -Sup«r Si-
Shell TS-2S8
I i ISOPBOaOKE
3-5-5-Trinaehyl-2-Cyclohajcan-l-On«
I ICAJUKMt TrrSAC3tCRI3E
Dov
EC; x»c!un«
?«rcalcron«sh«ii«! H«c»torin»i
I I
CTT/1RC3ESZEMB
Kooociiloro-3cnz«na> a«nznne-Oilpride ; Shanyl Chloridn
Ashland Monoc&loro B«CZ«Q«I Dow Konocnlors 8«nzs>i«
oth«r:
PI 1,2.4 -T
n!.».«.
Ethyl«n« Dichlorid*; Dow Echylim* 3ieaiorid«;
Olln E£!>yl«r.« 2ic!-.lorid«
n 1.1.1-a
M««hyle&loroforai 1-1-1-TC2; Cilorori:«n«i Vinyl
Tricnlori4«i l-l-l-Triehioro«tMn«i 1-1-2 TricJtloro«chanr
Oo« -Ciaoroeusnm- Htt! Qxloroeli«n« VO, SU»
X-Trichloro* ch«n«
"rri«thon«"j •3«nkl«n«"
I !bi»
I |
Trichlorcmaehan*
I Ij.Z - DI
O-Oiciiloratxnzxna t ?-Oichloreb«n=an*
Sov Ori-jjdieiioro 3cnz«n«
?ropyl«n« Dichlorid*
-12-
162
-------
sawarrs (Cone.)
CHLORIDS
Mathwu Oichlorid«> DicbloreoaeiiaiMt M««!tyla
Bichloride i M«thyl«n« bichloride
Dow P
D
Tri«l«n«t Tril«n«i Trichlorani Tric)Uor«n> Algylanj
Tartimr; Trilin«, Trij Tr»thyl«ni Trothylanai r
Chloxylant
LJ
OICHLORIDE
Oichloroath»n«; Glycol Diciiloridii 1,2 Dichloro»ch«c«i
Etbylan* Chloride : Ethan«-OC, 3-Dicl)lorid*; "Brocld*";
"Oaacnntol" ; "Borer-Sol"; "Di-<2»loro-«ul3ion" ; "Dutch
Liquid"; "EDC"; "2OT 1, 6S6"
D
Ethylan* Taeraeblorido Tacrlchloro«thyl«n«i Otrbon-
Oicblorid*! Oidakua, N«m«, T«txacadt Tscropil,
?or=I«n«, Ankiloseiai *B««-Solv"; "?«r-S«e";
"^ttreaaolv"; "Cow-Per"
a
HAPHTA (CCfll, TAR)
B«nzol ISO
'Company
Alcnn
Aacco
CSC
ad ,
Raic&hold
occ
(V)
Co* of CJUULCL&
™ Onion oil o£
- Air Products and Oxoaticals,
* '"cyronr'T^^I. Solvents Corp.
— Itoichhold Chgqic*l!f Inc.
- Varcum Ch«micaJL Division of
Kcicnhold Ch«ndcml*
— Onion Carbida Corp.
-13-
163
-------
-------
' . • ' . ' APPENDIX B
CROSS TABULATION:OF AGE OF INK MANUFACTURING
; FACILITIES,BY NUMBER OF EMPLOYEES
165
-------
-------
INK iNuusTRY SURVEY-
FILE : INK (CREATION DATE
= ;03/03/78)
G56 WATER PRESSURE USED FOR
COUNT
COL PCT
TOT PCT
! — IMTA = — =
C
101 TO 150 PSI
.:
51, TO 100 PSI
A
• Lii55 f.fAN 5D Hil
!
COLUMN
TOTAL
063
I
IT
I
I
—
I
I
I
.
I
I
I
-
I
I
s
i *
c
0
P
25
1
75
3
4
Tubs under 10
Water Use Per
0 50
0
.0
• U
.0
.0
.0
.0
3
.0
.0
4
.0
Q
I
-
I
I
I
I
I
I
I
I
r
i
i
i-
1 U 1U
B,;
; 0
0.0
0.0
0.0
1
, 3
12.0
30,. 0
3.0
; 7
70.0
7.0
10
10.0
I
I
I
I
I
I
I
I
I
I
I
I
I
I
i-
U h U b b
WATER WASH
-
T A H 'D L A 1 — I U N CT7 *
BY 063
»»•»»»»*«.•»»»»«»«•
Gallons
Tub Rinsing (Gal)
0 TO 5
A
100
1
1
84
24
, 21
36
74
64
86
"l
.0
.0
21
.0
.4
.0
64
.4
.0
86"
.0
r
• i
i
i
i
•i
i ••
i
i
i
i
i
i
i
i
HUW
TOTAL
1
1.0
25 -
25.0
74 /
/4.0
100
100.0
'—,
'
>
-
C56 WATER PRESSURE
'
COUNT
KUW HC T
COL PCT
TOT PCT
C
101 TO, 150 PSI '
d
51 TO 100 PSI
' • -A
Lt55 Tf-AN all HSi
COLUMN
TOTAL
G64'
I
li
TO
I
-I— •
I
I
I
r
i~"
i
i
i
i
i
i
i
i
L 1
0
0
U
0
2
50
(j
U
50
0
1
USED; FOR
Tubs 10 to 50
Water Use Per
u In
0
.0
.u
.0
,
1
.3
.0
• 7
i
.0
.7
2
.4
11 1 U 3U
I C :
I
I
1
I
1
I
I
1
I-
I
1
I
I
0
o.o
6.0
J
8,.3
•'21 '.4
eLtl
11
1 U . 4
78.6
7:. 6
14 -
9*7
I
I
I
1
I
T
1
I
I
1
T
I
1
I
I
1
v, « U 3 5
WATER WASH
TABU
LAT1CTN UP *
8Y Q64" v
Gallons ,
Tub Rinsing (Gal)
o 1 u
8
0
0
0
36
40
V
i /
59
13
22
10
0
.0
•°
1 j
a
.6
• u
19
• a
.4
.2
32
.2 •
u
I
I
I
1
I
1
I
I
i
I
1
I
I
ru t>
a
1
100.0
1*0
0.7
52. P ,
19.8
l3.d
76
79.2
52. P
96
66+7
KUYl
TOTAL
I
I
I 1
I 0.7
i
I '
I
I 25.0 :
I
1
I
I 107
I 7<*.3
I -
I
i
144
100.0
.167
-------
INK INDUSTRY SURVEY
FILE
INK
(CREATION DATE = 03/03/78)
f A a ITU"
CS6
•WATER PRESSURE USED FOR WATER WASH
'i'Ubs 51 to 100 Gallons
Q65 Water Use Per Tub Rinsing (Gal)
COUNT I
RtJW>tl lUVtK 1UU bi IU 1
COL PCT I 0
TOT PCT I E 10
C
101 TO
B
51 TO
A
Ltbi> I'
I
150 PSI I
I
I
-I-
1
100 PSI I
I
I
"•!•*
I
HAN STT'FS I. I
I
I
0
0.0
U.O
0.0
1
3.3
100.0
u.a
0
U.O
0.0
0.0
-L
COLUMN 1
TOTAL- 0.8
-JL-
1
I
L
I
1
I
I
i.
I
. I
I
I
— i-
0
0.0
U.O
0.0
3.3
33.3
o.a
2
66.7
i.s
3
2.3
J i
I
-I-
I
I
i
I
I
i
I
I
I
I
I
I
I
-I'-
ll 1 U D
C
0
0.0
U.U
0.0
0
20.0
24.0
4. (3
19
76.0
14.6
25
19.2
u o
I
—
I
I
I
I
I
I
I
I
Iv
I
I
I
-
1 U. iU
8
0
0.0
0.0
0.0
46.7
38.9
iu.a
22
61.1
16-. 9
36
27.7
BY G65
PI^ cr —
1 A
— — "•«» — "• — '
I 1
I 100.0
I
1.3
0.8
I 26.7
I 12.3
I
I
I
—
1 56
SSTfT"
86.2
43.1
65
50.0
TOTAL
I
_ f "— • '-"— ' •—
™ i
I 1
I 0.8 - x
-
I
I 23,1 :
I
I 99
I / rj > e.
I
I
130
100.0
!
A H U L
G56 WATER PRESSURE USED FOR WATER WASH
COUNT
kuw per
COL PCT
TOT PCT
0
OVER 150 PSI
d
51 TO 100 PSI
A
CESS THAN bU Vb'J
COLUMN
TOTAL
BY G66
TUDS 1U1 to 250 Gallons
G66 Water Use Per Tub Rinsing (Gal)
1UVLR 1UU 51 1U LO 11 TO b*"1 ' "~" "~~" " rr' c ^"^
I 0
IE ID 1C
I
I
1
I
-I
n >-•*-<
~I
-I
I
T
I
I
0
0.0
-1-
I
I
0
0.0
- i-
I
I
0
0.0
u a i u i u
I 8
- i— — — —
I 0
I 0.0
I
"•'
I
I
'0.0 i U.O i U.U i u.u L
0.0 I 0.0 I 0.0 I 0.0 I
u
0.0
0.0
1
I
I
|6.7
sn.o
1
I
I
I4*
46.7
38.9
i e
I 26.7
I 38.1
i
I
I
A
100
i
20
15
1
.0
.6
.0
.0
.8
O.U i
-------
INK INDUSTRY SURVEY
FILE
INK
(CREATION DATE =03/03/78)
G56
•'"*• * * » »..» tt a L H U ^ b 1
PRESSURE USED FOR WATER WASH
A H U L A [ i U N 0—F *
BY Q67 WATF
COUNT
ROW H<_ I
COL PCT
TOT PCT
D
OVER ISO PSI
51 TO 100 PSI
A
~ LbbS FHflN SCT PSI
COLUMN
TOTAL
-^ Tubs '
Q67 Water
I
IU
I
I
I
- I
I
I
«»T —
i
i
i
r
r
i
i
—
VtK iUO 3
0
E I
0
0.0
0.0
0.0
0
0.0
0.0
0 .0
2
3.G
100.0
3.S
2
3.5
-i-
I
I
L
I
1
I
I
1
I
I
I
I
— i—
i5JL: to 500 saxxons
Use Per Tub Rinsing. (Gal)
1 TO
C '.
0
0.0
1 0.0
0.0
.•1
6.3
25.0
i.a
1 3
7.5
75.0
5.3
7*0
1 0 i i I U b
I C
"I
I
1
I
I1 •
I
I
I
I
I
I
I.
0
0.0
0.0
0.0
o
37.5
46.2
1,0.5
*-" 7
S3. 3
12.3
13
22.8
U 6
I
I
I
i
I
t
I
I
I
I
I
I
I
ru 10
8
0
0.0
1 " 0 .0
0.0
'• , 2
12.5
18.2
3.5
9
81.8
15.8
11
19.3
"a
i
i
i
i111
I
i'
i
i
i1
r
i
i
TO 5"
A
1
100.0
• 1.7"
1.8
7-
43.8
25.9
.12.3
. 19
47.5
70.4
33.3
27
47.4
I
-1
I
I
r
i
r
i
i
r
i
— r
i
i
WOW1— "
TOTAL
1
1.8
— rs
28.1
40
— 70.2
57
100.0
(• + *•* *-»--*--*-T» ****.**.»» *. * .LnUSbTAbUL
CS6 WATER PRESSURE USED FOR WATER WASH
A r
BY
L 0 N U F '"••— *-
Q68 WATEi
Tubs 501 to 1000 Gallons
.-' C68 Water Use Per Tub Rinsing (Gal)
COUNT ,1
HOW HCT~l.oVtH IUO bi TO 10 11 IU bO 6 TO 10
COL. PCT: i o
TOT PCT I E I D 1C 18
\»3Q . ^»»— — — — — «.| -.^«— — — WM J>«>MOTM ^..
8 I 01 3
51 TO 100 PSI I 0.0 I 30'.0
I 0.0 1 60.0
i o.b r io:.3
A ., nr 1 — r 2~
LESS THAN 50 PSI I 5.3 I IQ'.S
I 100.0 I 40.0
-i-
I
I
1
r
-i-
-r~
i
i
2
20.0
66. f
6.9
T~
5.3
33.3
I 0
I 0.0
1 0.0
t 0.0
-I
~I T~
I 5.3
I 100.0
0
I
I
I
i
I
•I—
I—
I
I
ro b
A
5
50.0
'26.3
17.2
14
73.7
73.7
TOTAL
I
— 1
I 10
I 3^,5
I
— I
i iy • •
I 65.5 >
I
I 3.* i. fa.y i J.A. i j.4. i 4a.j i
•I -i— — .< 1.— 1 . -j . !
COLUMN 1 5 31 19 29
TUTAL j . * 1 I , '£
10. J
J«*
0:3.3.
tU.I.U
169
-------
INK INDUSTRY SURVEY
FILE
INK
(CREATION DATE =03/03/78)
G56 WATER PRESSURE
COUNT
ROW FCT
COL PCT
TOT PCT
B
51 TO 100 PSI
A
LESS T^AN 50 PSI
COLUMN
,U,«U
?j — g — 5, — 5-
USEO ?<
C69
I
"lOVh*
I
I E
-i —
I
I
I
-I—
I
I
I
1
-I-
12
5
9
50
3
10
TUDS over
Water Use
100
1
.5
.0
-3
1
.1
.0
*O
2
. 3
3
0
I
I
I
1
I
1
I
I
i
i IU
D
1
12.5
1 U 0 e U
5.3
•u
0.0
0.0
Q.O
1
3.3
I k U
DR. WATER
1000
Per
11} 1
I
— 1_
I
I
i
I
I
I
r
i
Tub
i ro
c
0.
u.
0.
18.
100.
10.
10'.
b b r
WASH
A
1
Rinsing
3
0
0
0
0
e.
2
0
5
2
5
u u
I
—
I
I
"I
I
I
I
I
• 1
1 U
A
75
31
72
57
!*•_
73
d u L A. r— r.-0-N ; u i-
8Y 069 . .
(Gal)
3 RCTS
TOTAL
I -
6 I 8
.0 I 42.1
. y •• 1
.6 I
I 1 i.
.7 I 57.9
.11
1
14 , 19
.7 100.0
i 170
-------
: . <• APPENDIX C '
CROSS TABULATION OF:AMOUNT OF WATER USED TO RINSE INK
TUB BY WATER PRESSURE OF RINSE WATER
171
-------
-------
INK 1NUUS1*Y
FILE
INK
(CREATION DATE ~ 03/07/78)
'•'. C-y
NUMBER OF
EMPLOYEES
AVERAGE NUMBER OF
•G10
COUNT ' I
K0l» PCT IOVER 30 21
CUL PCT I YEARS
. , -
'EMPLOYEES
AGE OF MANUFACTURING
! FACILITIES (YEARS)
TO 30 11 TO 20 6 TO 10 3
A T I 0 N
BY aio
-
TO 5 LESS
N 3
OF *
AGE
,TMA ROW
TOT .
: 'L I
- " " OVER "I5U I
I
, I
101 TO ISO • ; I
T
I
' ' ' J ' ' ' T'
91 TO 100 ; I
I
T
i r
81 TO 90 • ' I
'''•'' • 'I
- - , -'- I
-T
, '71 TO 80 ' I
» I
~T.
fj ' I
61 TO 70 ' I
I
T
«t.
F -•••.!
51 TG 60 T
'] i
rni IIMN
1
' ^5*0
1.6
8
86.9
1-3 5
ua
0
66.7
, 3.1
0 *t
. 3
75 0
4.7
0.7
I.
, 33.3
1.6
0.2
1
20.0
1*6
0 "*
0
0 0
0*0.
0.0
fit*.
I
T
I
I
- I-
I
I
• T
L
r
I
I
I
I
I
I
I
I
T
I
I
I
.1
T
I
T
I
I
-T_ T
o
0 0
0.0
0.0
0
0.0
Q, n
0.0
1 "
33.3
1.7
'02
; 0
0 0
0.0
d.o
i
33.3
I 7
0'.2
; 0
0.0
0.0
0 0
o:.o
0.0
AH
i
i
i
i
T _
I
I
T
I
r
I
I
j
I
I
I
T
I
I'
f
I
T
I
I
r
L
r
L
I
T in
2
50 ^0
1.6
0.4
1
11.1
0 i ft
0.2
0.0
0.0
(i j. n
1
per a
0.8
0.2
1
33.3
fl 4
0.2
3
60.0
2.4
n 7
2
£.£. t
1.6
0.4
i ik
— t «
I
L
I.
T T
I
I
T
I .
T
I
I
T
I
T
I
1
r t
i
i .
T
I
I
I
T
I
T •
I
I
T
"
1
3^ n
1.0
0.2
0
0.0
n n
0.0
Q
0.0
0.0
n n
0
n n
0.0
0.0
0
0.0
n n
0.0
n
0.0
0.0
efl
0
8n
0.0
0.0
aa
± —
I
T
I
I
• T -r
I
' I
T
I
T
I
I
T
I
I
i
i
T'
i
i
T
.1
T
I
I
I
I
I
^
0
n n
0.0
0.0
0
0.0
n n
0.0
Q
0.0
0.0
0 0
0
9fl
0.0
0.0
0
0.0
0.0
20.0
2.0
rt -5
0
Of\
0.0
0.0
en
— t- —
I
T
I
1
-r r
I
I
T
I
T
I •
i
T
I
T
I
I
i — ,
L
I
r
i
T
I
I
I ,
t'
I
r
*
0
Q 0
U.O
0.0
0
0.0
Ufl
0.0
Q
0.0
(i n
0
»A
0.0
0.0
0
0.0
(} ft
u.o
ll
0.0
0.0
o n
1
2.0
0.2
An
±
i
T -
I
I
I
I
I
T
1
I
I
T
I
r
J.
I
I
< 1-1 l-i l-
I
r
I
I
I
I
I
I
44*
9- .' '
H.O
0
3
0 7
1
J
COLUMN
. .' ' TOTAL :
(CUNT iNUtQ )
64
14. 3 ^
60
13.4
:
..,,.,.126
. 28,2
. . ,.,98. ..
21.9
. 50
11.2
•
49 4^
11.0 100.
173
-------
INK INDUSTRY
FILE
CCKEATION UATE =03/07/78)
as
NUMBER OF
EMPLOYEES
AVERAGE NUMBER OF EMPLOYEES
[
.,10 AGE OF MANUFACTURING
'•'JlifT I FACILITIES (YEARS)
BY (210 AGE .
HOW PCT IQVER 30
COL PCT IYEAHS
rn r or T r cr
E I
/• i Y n c n T
i
i
_T
0 I
31 TO 40 I
T
1 "-" ' ' - i
I
-I-
C I
21 TO 30 I
I
T
5 I
1 n -rn "an T
i
i
T
A I
LESS THAN 10 I
T
— " 1
I
COL- LIMN
2
15.i 4-
ol4-
3
12.0
*t t 7
0.7
16
27.6
25.0
13
7 n -5
20.3
2.9
14-
7.3
•> i 4
Ci 1 « 9
3.1
fi*t
21 TO 30 11 TO 20 6
T e rn T
I
T
I
I
I
I
r
I
T
I
I
r
L
T
I
r
—4-—
I
'I
T
I
0
0 4 0
0.0
0«0
i 4
16.0
6 7
0.9
i g
15.5
15.0
1-3 7
48.3
6.5
i 16
8.3
~in 7
3.6
' bQ
I
r
i
i
i
i
T
r
i
r
r
I
I
- 1 -.
I
I
T
I
6
4.3
1.3
6
24.0
't t 8
1.3
19
31.0
14.3
^ * u
29
•5-> 7
23.0'
6.5
57
29.7
(,q -5
12.8
126
I
T
I
1
-4—
I
I
f
I
T
I
I
T
I
r
i
i
i
i
T
I
TO 10
£
z
15 'i
2.0
0.4
9
36.0
g 2
2.0
lu
17.2
10.2
•3 n
30
30.6
6.7
46
24.0
10.3
aa-
3
T
I
T
I
I
T -r
I
I
I
T
I
I
T
I
T
"I
I
T
I
I
T
I
TO 5
g
2
15 *v
4.0
0.4
2
8.0
4 0
0.4
•3
•3.4
4.0
14
109
28.0
3.1
29
15.1
6.5
eo
LESS THA KOw
N 3 TOTAL
I * T
I
I
1
-4-—
1
I
I
T
1
I
,'T
I
I
I
I
I
I
T
I
1
7*7
2.0
0.2
1
2..0
0.2
- -9
5.2
6.1
U.7
13
10 ^
26.5
2.9
30
lb.6
*• 1 "
6.7
43-
I
f
I
1
— T
-t t-i i-t *
I
-r
r
I
I
I
j
1
I
I
I
T
I
13
2.9
25
5.6
55
13.0
128
— 3-S-.-&-
192
43.0
TOTAL
14.3
13.4
28*2
21.9
11.2
11.0
100.0
174
-------
APPENDIX D
PROCEDURES" FOR METALS ANALYSIS
BY INDUCTIVELY COUPLED ARGON PLASMA
175
-------
-------
Determination ;of Total Metals in Water
and Wastewaters by Plasma Spectrometry
CRL Method Nos. 504-570
Scope and Application •, .
This procedure is applicable to the determination of calcium, magnesium,
sodium, potassium, aluminum, barium, berylium, boron, cadmium, c-hromium,
cobalt , copper,, lead; manganese, molybdenum, nickel, silver, thallium,
tin, titanium, vanadium, ytrium and zinc in water and industrial municioal
wastewaters. j . ---•-.•
Summary of Method . •- - :
The sample .is digested with 8 N nitric acid to near dryness followed by
additional heating with HC1 to solubilize transition and noble metals.
The sample is cooled, diluted to 50 ml and analysed using Inductively •
Coupled Argon Plasma Atomic Emission Spectrometry (ICAP). The alkali
metals concentrations are expressed in milligrams per liter>-'-wh-ereas-
concentrations for other metals are expressed in micrograms per liter.
v:enty-two metals are routinely analyzed. • - ' "
, n equipment j - - _ ' . -.-••-.
Jarrell Ash Aiomcora.p 750. Inductively coupled argon plasma emission
spectrometer consisting of: i - - -
i. - : • ' ' • ' . '- '
a. KP generator ••:'•_
b. Plasma housing
: -1. Water-cooled induction coil • .
2. Quartz torch , , . • ' . .
3. Cross-flow nebulizer ^ .
4. Spray chamber ' ! . '
'< • ' V
c\ Direct reading spectrometer -
, 1. Entrance slit . .
2. Refractor plate at^entrance slit
3. Grating , . • . - • -
4. Exit slits ';• • ' -..'.. • • ;•
5. Phototubes. .;-..-
d. Computer for•instrument control ' -
e. Data output device. ' "•
300 ml tall form benkors ' '
Mettler PR 700 Balance ! ' . '
Corning Hot Pla'tes , "~
177
-------
Reagents/ Water, Glassware and Standards
Redistilled Nitric Acid '(1:1-8 Normal).
Hydrochloric Acid (1:1), Reagent Grade.
Glassware; Beakers for digestion, after being run through diswasher, are ;
rinsed with distilled water and placed in an aqua regia bath for at least two
hours. They are then rinsed thoroughly and allowed to air dry. The chemist'
performing the digestion will select his or her beakers and give each a hot
acid wash by following then with 1:1 HCl and placing on the hot plate for at
least one half hour.
The laboratory distilled water is passed through an ultrapure mixed-bed resin
column before use. 7J.1 water used [unless otherwise stated,-has been passed
through the mixed-bed resin (Super ;Q Water).
Standards: All standards are diluted from Fisher 10Ou ppsa Atomic Absorption
standards with the exception of silver and beryllium (variaii) and Yytriuru
(made from ytrium nitrate (Y(N03)3),.
iiandards used for the ICAP; Calibration Procedure
SOOO: Mixed-bed resin water (super Q water)
S001: Cne ppm in all elements except silver and
calcium
AGCA: 1 ppm silver and'10 ppm calcium, made fresh
daily.
1000: 1000 p^n calcium (-Fi-sher) • ' •
XXXX: .134-8 ppm j.ron (Fisher), FFFA matrix only.
ocedure ^ • ,
i. A designated al'icruot (usually 50 ml) of well-shaken and preserved
samnle (pH<2) is poured off into a 300 ml tall-form beaker. Normal
procedure is to place the beaker on an automatic-tare balaince and
deli.ver 50 g — drawing off excess with a disposable pipet. (This
procedure assumes the sample is, of sufficiently low concentration that
the specific gravity is not appreciably greater than one. The purpose of a
mass determination rather than!a volume one is to eliminate cross-contamina-
tion) . After the addition of 6 ml of 8N redistilled HNO3, to the
sample a ribbed be'aker cover is placed on the beaker and the sample
is heated to near dryness. (The sample is not taken to complete
dryness to avoid the loss of boron). .If the residue is dark colored
after cooling, an additional 6'ml of 8N HN03 is added and the sample
is reheated. This process is continued until no color change is
detected.
<>. Following the digestion, 5 ml of 1:1 HCl is added and the residue is
dissolved and/or placed in suspension by warming on a hot plate.
After cooling, the sample is transferred to a pre—tared' 2 ounce
polyethylene bottle and diluted ,up to 50 g. If some solids remain
undinsolved, the sample is filtered into a 50 ml volumetric and then
transferred to a polyethylene bottle for subsequent analysis,.
178
-------
3. Operating Conditions
a.
b.
c.
d.
e.
f.
Incident RF power
Reflected RF Qower
Plasma observation height
1.1' kw
mimimized (<10 w)
15 mm above load coil
Horizontal observation position.•.center
Aspiration Argon flow rate 0.6 L/min
Plasma Argon flow rate 22 L/min
4. ICAP Standardization Procedure and Sample Analysis.
Following startup, the instrument is profiled with the mereisry monitor.
The micrometer reading is recorded,on the sheet with the i^-terelement
correction values for the day.
The matrix is brought onto, core and time and date established. The
available matrices are: :
CCAS: correction for calcium
FEAS: correction for calcium and iron
KlAS: correction for calcium and iron and
outputs potassium.
The Q-string QEGGGA3 is se.t for standization. This string of commands
will erase the burn buf f er;s, execute three burns, average them, and
print the average on the teletype.
(It has hfeen f6~und that examining the -standards in-background mode allows
a better judgement of the'hois'e .in a given channel).
S. The standards cited above .are run. Once it has been verified that the
standards check, the value's for interelement correction for iron and
calcium are recorded and entered via the data base manager. In actual
operation it is possible that these may vary only slightly £5%) from day
to day, in which case they need not be entered.
Upon return to the operating system, the matrix is recalled, and the
blank and -1 ppm standard are checked. If these .remain with; in standard—
2ation, an instrument AQC 'solution is measured. (This AQG solution
is simply the waste from the drain of the nebulizer, collected and
held until it is deemed stable. The values for this solution are
recorded in a log book and compared with previous values. This is
a check .for gross operator error during standardzation..
6. Once these criteria have been satisfied, the instrument is rondy
to run samples. The blank and 1 ppm standard should be checked
every 30-45 min £0 establish that the instrument has not drifted.
The blank should also be checked if .values above detection limits
arc fo-und .for tho field blanks or digested laboratory blanks.
179
-------
7. S.tmplcs nro aspirated for 45 seconds before executing the Q string
'QEGC which perform a single burn followed by output in concentration
mode which-includes interelement corrections. Longer flush times,
nay be desired for ^samples which follow high (>500 ppcn) iron samples
or high (>1000 ppm) sodium samples. No other elements have been
encountered in sufficient quantities in real samples to result in
noticeable memory effects. j
8. Duplicates and spikes should be; checked against the corresponding
samples before continuing. This is to establish whether deviations
occur in the digestion or measurement of samples on the ICAP. If
it is found that the digestion is not at fault, restandara-isation
on the ICAP is recommended.
9» Saraples at high levels are routinely diluted 10-fold to determine
if results for all elements are valid or the result of i^tererence
not accounted for by the matrix ISCC's.
The paper tape from the teletype is read into the DG NOVA and the
report plus QC check is performed by programs written, in BASIC.
Quality Control \ •
Four typos of quality control samples are put through the digestion
process at the sane time as the samples. I-n a typical run of £0rty
samples there are in addition, four blanks, 4.AQC solutions, 2 dupli-
cates, 2 spikes.
1. Blanks: These are simply the laboratory super Q water carried
through the -s~ame digestion [process as the samples. Tr>e; blank
data is summarized periodically and is used to determine detec-
tion limits for the method (average and 2 standard deviations).
2. AQC Solutions: A series of solutions were made to cover the
ranges measured for each parameter. These were arranged in
Youden pairs approximately as follows: 10 ppm - 8 praa; 1 ppm -
800 ppb; 100 ppb - 80 ppb. Two pairs of these solutions are
digested as part of the run. This is separate from the instru-
ment AQC and calibration procedure mentioned earlier.
3. Duplicates: Two samples are chosen to be analysed as duplicates are
carried through the digestion process. The results for these are
expected to be within 10% of each other for each elenient, for concen-
trations in the working range (blank one -r 10 standard deviations).
f!: Two n.implo:. arc chonon to bn analyzed An npLkos. A table
of spike concentrations in'terms of final concentrat-ions is formulated
Spike recoveries are • determined if the sample is less than 2001; of
the cxcldorl spike.
180
-------
Routine1 Maintainance
Following four days of operation the torch and nebulization spray chamber
should be acid washed. Before the torch is removed and after it is replaced,
statistical programs are run to determine the standard deviation of all the
lines when aspirating blank water. Dark currents are also examined in this
manner. A reading of the profile1 meter is taken for'each element both before
and after cleaning while aspirating both blank water and the 1 ppm standard.
When the torch'is replaced, coarse alignment is made using a 1000 pom yttrium
standard to center the image on the slit. Fine' adjustment of the mirror is
made by maximizing-the signal to noise ratio on the lead line.
Once a month/ statistical programs are run.to maintain an historical record of
intensities obtained on each line for the series of standards.
Calculations ~.
These are done by the computer program .(written in basic) including
insertion of dilution factors to give results in mg/1 for calcium,
magnesium and sodium and ug/1 for the other metals.
Reference
1. Manual of "Methods for'Chemical -Analysis' of""Water and Wastes"',
U.S. Environmental 'Protection! Agency, Office of Technology Transfer,
1974, Washington, DC, pp 78-155.
' i i
2. "Simultaneous Multielement Analysis of Liquid Samoles by Inductivelv
Coupled Argon Plasma Atomic - Emission spectroscopy" , U.S. Snvironmu.ital
Protection Agency. Region V/; Central .Regional Laboratory, Chicago,
Illinois, (unpublished)..
181
-------
Ag
Al
B
Ba
Ca(l)
Ca(2)
Cd
Co
Cr
Cu
Fe
Name in nm
Silver 328.1
Aluminum 396.2
Boron J249.7
Barium 233.5
Calcium 393.4
Calcium 364.4
Cadmium 226.5,
Cobalt 238. 1
Chromium 267.7
Copper 324.8
Iron 259.5
Mg
Mn
Mo
Mi
Pb
Sn
Ti
V
Y
Zn
Name x i n nm
MagnesTurn 279.6
Manganese 257.6
Molybdenum ' 203.8
Nickel 341.5
Lead 220.3
Tin '190.0
Titanium , 334.7
Vanadium 309.3
Yttrium 417.8
Zinc 213.9
ELEMENT LIST AND ANALYTICAL LIMES ,
TABLE I
A list of the elements- currently analyzed by the CRL ICAP-AES instrument and
the emission line chosen for ;each element.
182
-------
Ag
AT
«3
Ba
Ca
Cd
Co
Cr
Cu
Fe
D.L. LQD :
ug/l ng/l
4 20 ;
7 35 .
3 15 '
i - 5 ;
<0.5 1 i
2 10 i
4 20 .. !
1 5 ,
1 5 ;
2 10 :
Mg
Mn
Mo
Ni
Pb
Sn
Ti
V
Y
Zn
U.L. LQD
ug/l iicj/1
<0 5 1
1 5
5 25
15 75
12' 60
12 60
1 5
1 5
~1 5
1 5
Five Runs over Three Months
' , MEAN*DETECTION LIMITS
AND LOWEST QUANTITATIVELY DETERMINATE CONCENTRATIONS (LQD)
; TABLE 2
The detection limit (D.L,.) is the amount of material that will produce-
a signal that- is twice as large as the standard deviation of the noise-.
The lowest quantitative determinate concentration (LQD) is 5 times the
D.L. and is the lowest concentration one can expect to report.
183
-------
-------
. APPENDIX S
•LIST OF PRIORITY POLLUTANTS
185
-------
-------
APPENDIX E
List of 129 Priority Pollutants
Compound Name
1. *acanaphthene \ •
Z. *acraleirr
3. *acrylanitrne;
£.. *benzane :
5. *banzidine i
ff. *carbon tatraichlorfde (tatrachlaraniethana}
*ChTorfnatad benazanas (othar than
dich-iarobenzanas)
7. chTorobenezsna
8. 1,2,4-trichlorofaanzana
9. hexachlarobanzane
1 *ChTorinatad ethanes (including 1,2-
I dicnioroecrtana, 1,1,1-trichloro-
ethana and hexachlorcethane)
1Q» 1,2-dichlaroethans
H. 1^1,1-trichloraathana
12. haxachloroathane
13. Trl-dichTaroathane
H. T,l,2-trichToroathane
15.. T,T,2,2-tatrachloraethane
t 11
16. chloraethana
*Chloroal'
-------
18.
19.
20.
2T.
22.
23.
24.
25;
26"..
27-
2S.
25.
30.
31.
32.
33.
"34.
bis(2-chloroethly) ether
2-chloroethyl vinyl ethsr (mixed)
*Chlon'natad naohtalene
2-chloronaphthalene
*Chlorinatad phenols (other than those
listed elsewhere; includes trichloro-
phenols arid chlorinated crssols)
2,4.',S-triehloraphenol
parachlorometa erase 1
*chl orofonn (trichlorcmethane)
*2-chloraphencil
*0ichlorobanzanes
l,2-dichlaroben22ne
1,3-dichlarafaenzene-
1,4-dichlorofaenzsne
*0ichlorobenzidine
3,3'-dichlorobenzidine
*0ichloroethylenes (1 ,1-dichloroethylena
and T,2-dichlorGethylene)
1,1-dichloroethylane
l,2-trans-dichlort3ethylene-
*OichloroproJ3ane and dichloropropene
1,2-dichloropropane
1,2-dichTqroprcpylene (1 ,3-dichloroprcpene)
"^^-di methyl phenol
E-2.
188
-------
*D1m'troto1uena
35. 2,4-dinitrotoluene
36. 2,S,-dinitratoluene
37. *l,2-diphenylhydrazine
38. *ethylbenzene;
33.. *fTuoranthene:
*Haloethars (other than those listed
eisswnere)
40. 4-chlorophenyl phenyl ether
I
41. 4-bromaphenyl phenyl ether
.42. bis(2-chtoroTSopropyl) ether
43. bis(2"-chloraethoxy) methane
; *Halomethanas\(other than those- listed
iTiewHere)
44. nsathylene chlorids (dichloromethane)
45. methyl chloride (chlororaethane)
45.. methyl bromide (bromamethane)
47.. branafann (tribrarnomethane)
43. dichlorofararaamethane
49. trichlora-fluoromethane
50. dichlorodifluoromethane
57- chlorodibrcmainethane
5Z. *hexachlorofautadiene
53. *hexadilorocyclopantadiene
54. *1sophorone
E-3
189
-------
55. *naphthalane
56. *nitrobenzsne
*Nitrophenols (including 2,4-dinitrcphencl
ana ainTcrocrasal)
57. 2-nitraphenql
55- 4-nitraphenol
59. *Z,4-dinitraphenol
60. 4,S-
-------
73. faenzo (a) pyrena (3,4-banzapyrene)
74. 3,4-banzaflucranthena
75. benza(SOfluoranthane 01,12-bsnzofluaranthane)
75. chrysene
77. acsnaphthylane
78- anthracene •
79w ; benzo(ghi)peryTena (1,12-banzapsrylene)
SQ« fluroena |
SI- phenatftrsna '
82. difaanza (a,h)anthracsne (1,2,5,6-d-ifaanzanthracane)
83. indano (l,2,3-cd)pyrsne (2,3-o^phenylanepyrane)
84:, pyrane
85". *tatrach1oroathylane
Sff., *toTuene ;
87. *trichloroathylane:
88. *viny1 chloride (chloraethylena)
Pesticides and Metabolites
89". , *aldHn
90. *dieldrin .:
i
$7. *chlordane (tachm'cal mixtura S metabolites)
*QDT and mataboTitss ,
9Z.. ; 4,4'-ODT '
95,. 4,4'-ODE" (p.p'-OOX)
94. 4,4'-ODD (p.p'-TDE)
E-5,
191
-------
*andosulfan and metabolites
95. a-sndosulfan-Alpha
96. fa-<5ndosul fan-Seta
97. endosulfan sulfata
*endrin and metabolites
98. andrin -
9Sv endrin aldehyde
*heotach1or and metabofi'tas
100. heptachlor
TOT. hejatachlor epoxida
*hexadrTQrocycTohexane (a'T isomgrs)
T02.. a-BHC-Alpha
TQ3. b-SHC-8eta
104. r-BHC (lindane)-Gainna
TQ5. g-SHC-Oelta
*po7ychtorinatad biphenyls (PC3's)
1QS. -PC3-T242 (Arochlor 1242}
T07. PC3-1254 (ArodiTor 1254)
.PC3-T221 (ArooHlor 1221)
PC3-1232 (Arochlor 1232)
TTff. PG-6-124S (Arochlor 1248)
m.. PC3-12SO (Arochlqr 12SQ)
112. -PCS-IOIS (Arochlor 1016)
113. ~*Toxapheife ~"
114. *Ant1ntony (Total
115. *A:rsenic (Total)
£-6
192
-------
'its.
117.
us.
119.
120."
121.
122.
123.
124..
125.
125.
127.
123.
125.
(Fibrous)
*Saryniu» (Total 3
*Cadnriuni (Total)
*Chrosriura (Total)!
*Copper- (Total)
*Cyanide (Total) .
*taad: (Total)
*Mercury (Total)
*NicxeT (Total) ;
*Seleniunt (Total),
*SiTver (Total)
*Thallium (Total),
*Zfnc (Total) ;
**2,3,7,ff- tatrathlorodibenzo-p-dioxin (TCDD)
*Specific csmpounds and chemical classes as listsd
in the cansant degree. ;
**This compound was speciflcalTy listad in the consent
degree. Because of the extreme taxi city (TCDD). We are reccroending
that laboratories not acquire analytical standard for
this compound.
193
-------
-------
' APPENDIX F
LIST OF SAMPLING CANDIDATES
195
-------
-------
, APPENDIX P
t ' .. '
LIST OF SAMPLING CANDIDATES
CATEGORY •! - Paste Ink Only
Capitol Printing Ink Co.
806 Channing Place, NE
Washington, DC 20018
Inmont Corporation
4700 Paddock Rd. ',
Cincinnati, OH 45229
CATEGORY 2 - Paste Ink Plus Water Flexo
Braden-Sutphin Ink Co.
3650 E. 93rd St. ;
Cleveland, OH 44105
Morrison Printing Ink Co.
4801 W. 160th Street
Cleveland, OH 44135
wikoff.Color Corp.
410 So. Gardner Ave.
Charlotte, NC 28208 i
Roberts &t Porter, Inc. - .
1001'Morse Ave.
Elk Grove Village, IL 60007'
CATEGORY 3 - Liquid Inks '- mostly solvent, some water
C - P & W Printing Ink Co 'f
3389 Powers Avenue
Jacksonville, PL 32217
American Inks & Coatings
P. 0. Box 217
Volley Forge, PA 19481
Richardson Ink Co. :
3901 W. Rohr Ave.
Milwaukee, WI 53209 |
J. M. Huber Corp. I
Raritan Center
Edison, NJ 08817 ''.
Thiele Engdahl
6699 Winthrop Street
Addison, '.IL 60101
197
-------
CATEGORY 4 - Paste Inks, Liquid Inks.- broad product mix -
(heterogeneous)
Flint Ink Corp.
25111 Glendale Ave.
Detroit, MI 48239
A. J. Daw Printing Ink Co.
3559 So. Greenwood Ave.
Los Angeles, CA 90040
Sinclair & Valentine Co.
5560 Doolittle Rd.
Jacksonville, PL 32205
Sun Chemical Corp.
3301 Hunting Park Ave.
Philadelphia, PA 19132
CATEGORY 5 - Speciality
Colonial Printing Ink Co.
180 E Union Ave.
E. Rutherford, NJ 07073
K. c. Coatings
500 Railroad Ave.
N. Kansas City, MO 64116
Naz Dar Co.
1087 No. Branch St.
Chicago, IL 60622
198
-------
' APPENDIX G
SAMPLING PROCEDURES
199
-------
-------
PROCEDURES '
Following the selection of sampling sites, final preparations
were made for the field activities',. The sampling protocol develoaed
by EPA (Draft EPA Sampling Protocol for Measurement of Toxics , '
October 1976) was used as a basis -for sample collection. However,
due to the nature of wastewater treatment at the sites selected,
some modifications to the EPA protocol were required. These
modifications, which were approved, by the Project Officer, are
described below. Additionally, all samples analyzed for toxic
substances were run 'in accordance with EPA Draft Analytical Protocol
for the Measurement of Toxic Substances , October 1976. ~
Protocol Modifications ;
The protocol developed for priority pollutant sampling recommends
the' collection of composite samples. Since, at three of the six
plants visited, ink' process wastewater is collected over a period
of time in holding tanks, the recommended composite sampling
method was not necessary.. At the remaining three plants, conroosite
samples were taken at the discharges from hot caustic' tub washers
on the days that they were operating.
l
Besides the collection of grap samples, some modifications of
che protocol's sample preservation methods were recuired. In
order to correlate the data between this sampling program and the
one conducted during the 1976 study, the preservation method
recommended in the protocol for the phenol fraction was changed.
The protocol shows phosphoric or sulfuric acid alone being used
for phenol sample preservation. For the 1976 study, samples were
preserved in accordance with the guidelines established under
section '304g of the: Act (Methods for Chemical Analysis of_ Water
and Wastes, U.S. EPA, Monitoring and Support Laboratory, 1974).
Specifically, the phenol fractions; were preserved with copper
sulfate plus phosphoric acid. To maintain uniformity, cooper
sulf ate and phosphoric acid were also used to preserve phenol
samples collected during the 1977 sampling program.
An additional, variation related to the protocol required
precautions against the presence of residual chlorine in samples.
Sample fractions collected during the 1977 sampling program were
not checked for residual chlorine in the field*. This procedure
was deemed unnecessary because all' of "the plants sampled discharge
to publicly owned treatment works precluding the need for effluent
chlorination. This fact was. verified in the field by the sampling
teams.
201
-------
Sample Collection _
Table G-l summarizes the number of samples taken at each site
during the 1977/78 sampling program. The four possible sampling
points at each plant were as follows:
(1) Intake Water or plant water supply - These samples were
collected and analyzed to obtain background measurements.
(2) Untreated Wastewater - Tub and equipment cleanings.
Composite samples were taken of the water rinse discharge
from hot caustic washers at three of the plants. At the
other three plants the untreated wastewater was collected
in holding tanks prior to outside disposal or discharge
to the sewer. At these plants, grab samples were taken
from the tanks after! the wastewater was mixed to ensure
a representative sample for the collection period. The
length of collection period ranged from a few hours to
over two weeks, depending upon .each plant's production
schedule.
(3) Treated Wastewater -L At five of the six plants the
untreated wastewater was combined with other plant waste
streams (e.g., cooling water, boiler blowdown) before
treatment or disposal. Consequently, no treated waste-
water samples were taken at these plants. At the remaining
plant, a composite sample was taken before the treated
wastewater was discharged to the sewer.
(4) Sampler Blanks - Deionized water was run through the
automatic samplers prior to taking composite samples.
This was done to ascertain the amount of hydrocarbon
contamination introduced by the sampler tubing.
At two of the six plants, more than one untreated sample was
taken to account for possible variability in wastewater composition.
After the samples were taken, they were properly labeled, packed
in ice, and shipped to the appropriate laboratories for analyses.
In most instances, the samples were shipped by air freight and
received at the labs within 24 hours after sampling. A chain of
custody forms, signed by the samplers, accompanied each set of
samples back to the labs.
Inventory of Sampling Points
Table G-2 presents pertinent information regarding each
sample taken during the 1977/78 study.
202
-------
TABLE G-l
NUMBER OF SAMPLES FHOM EACH INK PLANT
Plant
7
10
19
21
22
23
Total
Type -of
Treatment •
A
B
. A
A '
^sTc,^)
B,C
Type of !
Samcle
Grab
Composite
Composite
Grab
Composite
Grab
Intake
1
' 1
1
1
2
1
7
Dntreated
2
3
1
1
2
1
10
Treated Samnler Blank
1
1
(D
2 4
Type of Treatment
A - None ,
B - Gravity Separation
C - Settling and Clarification
D - Neutralization
203
-------
1977*1373 Inventory of SaispJ.* Poin«
Paint/Infc Indtiicry
Bums, and Boa/Richardson Asoociacaa SaapLiag Pragma
1-1-tl
1-l-r
l-L-t
1-Z-*
1-2-T
1-3-il
1-3-t
2-1-t
1-1-*
2-1-S
2-1-a.
2-3-R
2-3-1!
2-3-S
Z-4-fl
2-4-f
!•-+••
3-1-11
3-1-1:
3-l-S
3-2-R
3-J-t
3-2-3
3-3-«
3-3-1T
3-J-iI
4-l-a
4-l-t
4-1-T
4-1-3
4-2-a
4-2-t
4-l-S
4-3-fl
4-3-t
4-3-S
3-i-a
5-1-t
J-l-C
S-l-S
3-2-*
5-3-R
s-3-r
5-3-3
5-3-*"
s-s-r>
5-3-5*
S-l-R
Srl-t
S-l-t
5-1-5
6-2-X,
5-1-T
6-Z-S
S-3-R
4-3-S
7-l-R.
7-2-*
7-2-t
3-1-%
3-1-t
8-1-3
3-3-R
3-Z-t
S-Z-T
3-2-S
8-J-*
a-i-i
9-l-R
3-1-1!
9-1-S
3-l-S
9-Z-a.
t-Z-S
S-A-001
S-*"01S
S-t^OOl
3-L-O02
3-1-004
5-8-OOS
5-C-016
3-0-017
S-G-021
5-4-022
5-«-023
5-?-O2*
S-T-02S
5-T-026
5-HT-067
5-HT-36&
5HT-OS9
s-r-ooi
5-?-O02
5-JMJ03
5-^-O04
3-3-013
5-S-019
3-3-020
3-f-027
!-r-o:a
5-?-029
s-r-oos
3-7-004
5-0-003
5-C-007
$-r-o30
s-r-03l
5-T-O32
S-f-038
S-f-037
S-F-031
s-r-oo9
5-r-oio
s-r-ou
S-F-O12
s-r-ou
J-f-033
3-r-034
3-r-O35
j-r-oio
j..f_^43
5-f-064
3-C-040
5-C-039
3-C-041
S-«-
-------
ttff A (Canr.)
3tft Cad*
9-2-3
9-3-R
9-3-T
9-3-3
10-1-R
10-1-1
10-2-R
10-3-R
U-i-R
U-l-t
12-l-R
12-1-t
U-l-R
13-1-1
13-1-T
13-1-S
13-2-R
ia-2-r
13-2-S
13-3-tt
13-3-T
13-3-S
14-l-R
14-1-1
14-1-1
14-1-S
14-2-R
14-2-T
14-2-3
1S-1-I
is-i-a
IS-I-T.
1S-2-R
1S-2-T
13-3-R
1S-3-T
16-t-R
16-1-1
17-1-R
17-1-t
17-1-T
17-2-S
17-2-T
17-3-n
17-3-rT
18-1-R
18-l-t
18— 1-T
13-2-R
1B-2-T
18-3-R
18-3-T
.13-3-6
19-1-R
19-1-1
20-1-R
20-1-:
20-1-t
20-1-S
20-2-R
20-2-1
20-2-3
20-3-R
20-J-T"
21-1-R
21-1-1
22— 1-tt
22-1-1
22-1-T
23-1-8.
23-1- t
SESA Ceda
5-a-oos
5-C-O48
3-C-OS2
5-C-OS3
5-C-040
5-C-041
S-C-O47
S-C-OS4
5-C-06S
3-?-066
s-r-070
5-r-on
S—S-O10
3-S-Oli
3-»-012
S-a-ou
3-C-05S
S-C-OS8
3-C-037
5-C-OSS
S-C-039
S-C-060
S-a-OM
S-a-oiS
5-3-016
S-a-017
s-s-ois
s-a-019
3-3-020
s-a-021
5-S-022.
5-^—023
S-S-024
S-S-025
S-a-026
S-H-Q27
5— ff*O28fL
5-H-029S.
5-S-O2E8
5-B-029S
S-B-030
S-B-031
3-S-032
S-C-064
S-C-065
S-g-033
3-B-O34
S-C-063
S-C-073
S-fi-037
S-J-001
S-rJ-002
S-J-003
- S-C-061
S-C-OS2
3-C-066
S-C-067
3-C-068
5-C-069
5-C-070
5-C-071
3-C-077
S-B-038
S-fi-039
S-S-035
3-3-036
5-e-ooi
3-S-002
3-E-003
5-•— ^ Cassnad
g»««j< Cassiad
Eire 1S449213
g,^^ Car-i«d
Hand Cazriad
COO on ;r*Mrra
-------
T3SL3 ?-2
PAST Bi S»V BXSXXaa. OFTICZS SMCTLIHO ?3CG2UM
ana
2
2
2
2
3
3
3
3
4
4
4
4
3
3
3
S
£
t
4
7
7
12
12
12
12
22
22
22
22
24
24
24
24
24
24
24
24
23
23
23
23
2S
28
26
2S
25
27
27
17
27
27
28
28
3*m
3. •*
T -
3 -
KB-SCC*
00215
00214
00216
00217
0012»
00128
00130
00131
C0119
00118
00120
00121
00082
000*1
COQH
00084
00113
CO 112
00114
00115
OOO89
000(7
00123
00122
00124
00125
11* 7oiBts
Raw Vasxawacaz
TXaacad XUCM
51ui$?«
Ta? Uaear
Rational Saapl*
08-OS-OU9S02
08-OS-OU9SOI
08-03-OO9S03
aS-03-OU9S04
08-03-O129302
08-OS-CMZ9S01
OS-03-OS9303
Oa-OS-OB9S04
O30S02
C330S01
O30303
CU0304
O01S02
001301
OOIS03
C301304
C331302
C331S01
C331S03
031304
08-OSHB61302
08-OS-M19J03
aa-os-E6i9504
SOI
3O4
309
3O2
SOS
303
SOS
307
1320 ;
1321
1S23
1524
1223
1319
1311
1344
1343
0803EG1S302
080SBHB301
08051013304
080SZC1SS03
OSQSEG1S30S
PS- 1
wear
I
I
s
a
I
T
S
ft
t
T
3
a
I
T
3
a
I
y
3
R
I
a
r
T
3
a
I
t
s
a
T
I
a
T
a
T
3
a
7
a
T
I
a
z
T
S
a
t
T
3
L
a
i
10/3/78
10/4/78
10/4/78
10/3/78
10/3/78
10/3/78
10/3/78
10/3/78
10/S/78
10/6/78
10/6/78
9/19/78
9/19/78
9/20/78
9/20/73
10/4/78
10/4/78
10/4/73
10/4/78
9/19/78
9/19/78
10/S/73
10/3/7S
10/6/78
10/6/78
10/11/78T
10/11/78
10/11/78
10/11/78
6/2S/78
6/27/78
8/27/78
8/27/78
6/27/78
6/27/7S
6/27/78
8/27/78
7/11/78
7/11/78
7/12/78
7/12/78
7/12/78
7/11/78
7/11/78
7/14/78
7/14/78
3/16/7S
8/1S/78
8/21/78
3/18/78
3/16/78
1/23/78
1/25/7S
Baza* and 3o«
ET -Howard n
Ml - Mark Sadc
H3
M3
MS, PS
MS, IS
MS, PS
MS, PS
M3*JS
M3,P3
MS
MS
MS
MS
MS
MS
S3 ,39
MS.fS
XS.iS
MS,;S
MS
MS
MS, 73
H3.JS
MS
MS
MS
MS
M3
M3
PS
PS
73
PS
PS
73
73
PS
MS
MS
MS
MS
Of
er
?«raenn«l
lilac
nraki
?!l - Paul scorch
EH of tta
SM ovganic ^"^*
EM mo«iv«d by
CM 12/13/78
£H
EM
EM
33
S3
S3
S3
HK
WK
«C
VE
SB
S3
S3
sc
•nc
HC
S3
S3
SB
S3
C3
C3
at
C3
PCS
?<•
?G
pa
7^
pa
pa
7G * On* slud^a samp]
GO rapnsancs aj^ 3
G3 batcfaa* o£ vtr.
SD
-------
; APPENDIX H .
ANALYTICAL DATA FROM INDIVIDUAL PLANT SITES
207
-------
-------
LU
i-
-t-[—
iiiiiiiiiiiiiiiiiiiiiiiiiiiiiii
zzzzzzzzz
3 33 333333
^(-•-•-i-l-r;!-;-
zzzzzzzzz
O LU
Z CO
UJ
X
to
i- en
zui
LU _<
zsz
-JI Z)
u.
It's
zzzzzzzzz
333333333
I- 1- i- i- t- I- !- •- .
oooooaoco
z z z z z z zz z
_
_• -H-l— I— f^l— f— i— H-Hr-i— h- i—>— r-)— t— >->—(— Ki— 1— p-f— f— «
oooacooooaaooaaoaoooooooaaoob
zzzzzzzzzzzzzzzzzzzzzzzzzzzzzzz
. >-h-}— (— i— i— f— i— :— r-i— :— f—i— I"*— J— H-f—(— i_i— u. i_i_
o a o o a o o CiO oo-ooooooaoooooociboaboo
Z Z Z Z_Z Z Z Z'Z ZZZZZZZZZZZZZZZZZZZZZZ
a
z
LU
C£
Z 3 LU >-
_1 3 i-i t£. a Ci
_J <-< Z LU >-< 3
v z o u_ z a u
a: a ci o. c -i M en en
CD CD _l _J
z z a o LU • en
^cn^coco_jen3
LU _J to i-i en en
en a a * * h- I-H
' -izi-icnciL^ ->-i-_ji-3Li:o
u_j_i<:zz:oooiT-HL-^(--i
z en en i- M '
Tiii -o r^.m ,
•1 PJ M H PI
f
rsrsrsNrsrsrsrsrsrsrsrsrsrsrsrsrsrsrs
^^
i
_l CD
1 Z
CD -'
MANGANESI
CALCIUMd
MAGNESIUi
rs rs rs
•^
iaJ 3 3 Z
h- a l-l 1-4 3 Z
z _i iii z a i-i 3
O *£ >- >-en
rsfsrsrsrsrsrsrs
. -i EN i-i Z •-
Ij.
U5
>- LU
.
Li Z
a -
z
I
-------
c;
01
I-
CO O O '
T* I V '
I _J -I _J
u
SZEZZSXZZZZZZZZZZZZZZZZZZZZZZ
ZZZZZZZZZZZZZZZZZZZZZ
u;
i-
en
^ ui
^ >-
-10
<: z
>
O LI
C CO
UI
Li
: zz z :
3 :
;zzzzzzzzzzzzzzz z-z z
1333333333333333333
z-
en
S
O, Ul
Z I-
~
Z
Ui .
3.
u.
z
O
F)
M N in O
T-H Q TH O- 0-
o o o
ro M TI
o . UJ X Ul
Z Z O.I-
- to ui <: • x
X I-
UJX
XCu
Ul -J
Z >• _l
UJ X >-
_]!->-
t UJ 3
X I «
I- N 1
X — Z
u. en i
->
« >-
_i ~
•C I-
X Ul Ul
t- z o
X Ul C£
a. a: O
x _J
_i >- x
>- 2. U
x -i XUl
a a. i-
zulr
O >H _j 3
C Z _J >-
M Ul >- Z
h- en cc Q
z ci: ui -iDD
_. 2 « eb eo o ^ -.- •
i w a H. zrx:i:«_i_l_i_i-ii-_j
o >-
u u
3~.w^. -lU|l-lX^-tlXCiejH>OI— )— t— h- HI>^- t Ul
a u a
Z ^ CD
>- .01
«r *o o
•cnin-ocnO'-iiiTr'«'rinrsc3i
•^tf3*O«otsCOCOCO^i—4TH*H-
• O ^ PI 1*3 T in *0 N G3
I PI PI PI PI PI PI PI PI PI
CJ PI M PJ CM CM M CM PI CM PI PJ PI CM PI CM f-l PJ PI PI P-l PI PJ PI P-l PI PI PI PI PI CM PI PI PI PI PI PI PI CM CM PI PI PI P,l P4 CM PI P-l PI PI PI PI
O <:
>-i CO
C£
Z
CL
Ci. Z
.- a
Z uj
-------
i
S iiIll5iiiiilIlIi-Ii§iii5si = 3555555355.3~£S3S35553335S = SS,S3 = = 35~S = 3 55S3SS5S33 =
H 2255S55225;s'222555£55£225:£555-555S2552.2a:2£:25 5*2 22*5 255-^55 5-2 2 555 22252 5525255222 ^
2 iSiiiziliiiliiiliiiii'IIIiliiilijiliiliglllililiiiliiiiiiiiltliiil iiililllli -
fs'.Ij - • *"
" ~ f . i ..?..-..*, • _. • . _;
_. - . -; . h - . . . . .
>j ••-• • r •;.-• ' ./', . .• i
.'.',' • - , . ^
Hll§§ = 5§B§l53H§l§§§HllH3§------s — 5 S S S SS3S55S55 5SS3HS53 S55S5S55SS53S 5555555=55 §
-.ZrS^IEHSilSS^SSSS^S^SsS^StsSE^SS^S^ESS^KijSSSSSSiESSS-SSSSSSSHsSSS^:!^^^ 2222S55522 -
z'-siiiiiiiiiilllli'iiiiiiliiilii'iilililiiiiliiillliiiliiiliiliiiiil iliiliiill \
-5cc^o> o-rco- ocor. oooo^ocoooooosoicoiiocooooo-.o-cc«o-«.i;c-' s. — ^ — ^i -3 tj ri — -« c —
= - — - « ' w o* z z z z — o o 3 o si — — o ' o u- > -v. v.- .- — -^ r. - ,-. -^ -i = ri , K ^ -
— — _ -• "i . n -o« r-i r-4 . - *n n v a rj r-i s- rx ii =• r. •*• L* -•; — — . t~ <-: ^
_— ^ « i-,_ .—""
-" ' " ' . - - %
3 -j — -c
• s s: :s u _j u i— _•>
5 i= :
~ S3 ~ •
; - c-: - -j-
s;2T5-SuiH2=.= H5S-S-iJ,zs =
Hfi^M-rTii^t^^tT^^EfsJ
s = =:
Z = 9tH;n^C~~'w~'"""~'
-| = = i=iM
— c £ - r u z 3 5 S ^.— ^ > 5 "*
I -c -"v a > t: ^- •> u
- - -
211
-------
Ul
H-
«
*rQ aooaonoooooo-o
i ti I «r to is I i t .1 i 0 CM -< CM rs m CM o
inz z zz z~ -. >- H- J— i- f— h- V- f— >_>_(— H- S— i— i— I— f— r— h- I— (— !— H- f-f— r-f— f— !—
G'OOCOOaOOOOOOOGCaOOGOOOOGOaGQGC
zzzzzzzzzzzzzzzzzzzzzzzzzzzzzzzz
N! U
^ ^-
_i a
tn
I-U)
zui
li
u.
U.-I
Ul X
c
en
1-
1-3
Id
-J-C
u.
z
:zzzzzzzzzzzzzzz
133 333333333333"
t- I— I— I— I- 1- S- I- h- !— f- I- I- I- I- I— I- (- I- 1- (-
aaoGooaaaoGooooooooo-
zzzszzzzzzzzzzzzzzzzz
WOOnOOaO-iCMaolflt.1000000.*
o -< -1 ri o i i o
ro M CM n ^
Ui
r—
10
i-
G
z
k!
N!
z
•c
G
z
•I
Ci
uj a
£4 UJ
D 0)
2 i-l
_J
_J
111
z
1**
Ul
a
ct
•IE
-TRICHLI
U] Cl
N "
Z f
Ul ^
a -<
*-(
i:
CS
O
l_
r->
cc
o
_i
D
M
w
Ul
_5 a
>• *•*
X C6
t- O
Ul .J
O 3
go
siz1
u ki
s>
»-l p
- Ul
0- T
UI Ul
z z
— — ^ t
?— t- o
Ul U1Z
£ 3Z Ui
o ozz
31 ES-
0 O G
CS £C ££.
a coo
O M -I
cc ax
o o cj
_i o: ^fe
"1— N 5^ Z) E
Lti 1 ^r,J^™G"3££&LiQ_*X^il£
^ t—t »> O 21 ''^* i * t vo^'iiTfs'CDCsoTHnm
ooooooooooooo
J^ J-J J
«.
1
to
r
•^ tn
• ui _i
tn o
. <: z
^, ^ ^, ^ UJ HI
3; i: t- i i i ca t
3 3 t-i g ts ea
jjzui-J S^5" *
2: tn 'tn f N
T n >o N to
M r-i r-i n CM
3OOOOOOOOOO
_I
1
G
z
en
L SOLID
1-
G
0
^> ^N
«J ^1
1. 1
G tO
Z Z
cn crs
hH >-»
1 1
O O
tn cn
cn &.
tn tn
a tn
„
o o
_l _1 _J _! -1
_l
1
CO
*^ !- ' 1
tn
t_(
_i
G
tn
» *-^
tn _i
3 -^ 1
tn _i G
i 3:
a >-. 3:
_l Ul'C S ' 3'
03; tn — 3 z 3:r:
>3 UIZi-i UJ 33r
zz: =3en KC. w M 3 r:
_|M3 - <:<£&>-<
!-3ii:oz-jGi:a-JZi-2:-a
O_J-en
ooooooooooooo oo
G *it
Q.
tr, '
>- Ul
^— «J
o; E
o <:
M U3
££'•
Cl- >-
.c.
i -
2 "~
5
z t.
212
-------
IIIIIIII III IIIIIIII fill IIIIII 111'IP 11III
r- r- ?— V- 1— i— H-i— H-l— f— r— r-t— r- iV- !— i— i— p- i— r- W «- f— H i— i— rC j-: J—" {— p- t— V-'h- I— r- (— V-
QQGOOOGOGOO c ooaooccccooooo aao o oo GCO a Q a <-• in
Z2Z2Z ZZZ ZZZ Z ZZ ZZZ 2ZZZZZZ22 §.§2§ §§ 5§.§ §§i S§
222222
a
3
_l
0)
~ a
-JO
'
OGGGGCoobGbabcabaoGGOQOooacGGobaoGGQOoab
222222222222 22 2222222222 22222 22222222222
; ^ - , .:.... , .
X . .
: ' ' ' -
\
5 S 5 55 2'22 2222 2^2 2 22 2222 222 222222 222 222 22 22
.333333333333 33 33333333333 3'3 3333333333333
EKiKKCiKctfijEKCirtt: K.O: ci Ciii: ti a: a. &. tc. v. te. &. &. a. u. a. sz tc. se. se. tz sz te. !£-z. a. c;
t- !- i-!-!— 1— >-l— >-!— j-i-i-*-!— 1-!— r- (-!-!— l-j-l— '1-1-!- >-H-r---l— i— j-r-i-f-l— r-r-
ZZ2Z222222Z222222222222Z22222222222ZZZ22
- ' • ~ -' -•''--.
- _ ' '
UTIlTOOOOOOOOb-DOOOOOOfOPJOOOOOOOOOOOO^^OOOOOOOO
pi PI *-» CM o o PJ o PI in PI *-i *-i o »-( o o ro cs o si ~.I3 3i C1 ;c iiitou.cnQcn— Ji>3 ui XT *-< bj ID^DT:
SU^^D^y >- 13 p OCOO ;UJ. •-( 2 3= - S 3 tn KG w »-i 3 C
x:3:^j^jguj^; DUJEUJ«J v^-w <£<±<:- « « a *H
H cn a: a-ce Ci.<:- UJ
(— _l
I-* li_
G -
2
1 -
O 1-
G
>-i »-j
i C£
2 i.
213
-------
cz
Li
a.
-!-l--i-(---
gggggggggggggggggggggggggggggggggg-ggggg
a
ui
z
Ui
LU
N
r in
Ul w
_
-f— •— cn(—^h-- LJ
i— _i
1-1 a.
i
LL.
0.
•^ Ci.
Z UJ
<: i-
z u
k- UI
in ul
01 C-i
UJ
_J 1-
I O
_! Z
u zi
ui _i
ui o
a a.
i- >-
o )-
ooooooooooooooooooooo;ooC'OOoooooc
ooooooooo
o
z ~sL
214
-------
UI
I-
•
O UJ
z: cn
UJ I-*
a: 3
UI
z
3
cn
i- cn •
2 UI
UJ _l
3 2
1 -•}
u.
U. '
UJ N
CD
01
^-"
t-t
2'
H~ 3
2
UI _1
3 _1
,-l «
• u.
2
1
1
1
1
I
1
UI
i- '
UI
g
tt
a.
Cu.
f.
' cj
i
m
t-
2
• • • .„
' ,
*
222222222222 2' 22222222222222222222 2 2222
3 3 3 3 3 3 3 3 3 3 3 3 3 3 3 3'3 3333333333333333 3 3333
. .
oaaoabaooobosbaaoaaaaoaobbaboaoooaaabb
22222222222222222222222222222222222222
/ -
i
_
O I O 1 fO G* O T"* *O in T CM CN '-I C*-I O O *0 O in CM *-t 7-* O *-t 0- O -z>-uj , . • s s o o ui • cn
cj3xt-z_i — cn — cncn_icn3
- , • ,- uj_icn wcncn
££UIZZlX-UIZ - cnOa->r-»H
t-2u_i OH- " " <:2wcno.-2o o x • tn_ij_jazo«-i3auios
i ?: X i- *- ui j cc v 3 T: z z . i- i i i o t w a co ^ _i :• 3
UirJLUUJ UIUUZUJOSCJMC3 Ul >- 3 3 i-HCDOCT >i Z
z-is_i_i i o-i_i3'-iii:a tt-i-HCi:!-! 2z:i:z«>_i_j_j_i_ii-_ii-i
uj CN -J vc ri i c: Z=-.az£iZiUwU)>-SOil.20UiiUi»iJ'0«aCiCJ_JI-l^H.|-"*_J!-3
2 -fi-(2Ulu3iiC2C::UJ-LJUJi-iUJ»~lZ>-»Cl_iIiCJh-Of— H-f— Ht— >i— co n -o r- -CS^C^O~^CS>:CS^a-C^CSCSO-C>.C>.CSCSC>-CSCSCNCNCSCSCSC>CS^C>-CSC^CS
2
3
0
2
2
o
2
o
o
r-j
s:
^^
^
^f
St
^
2 2
2 Z5
f< a^
Q 0
2 2
2 2
3 3
o a
2 2
o o
o in
c
UI
Ul
2 O
C 2
^ z
cs o
2
3
0
2
2
3
a
2
o
o
c
^
.J
I
CD
T.
3
CJ
_J
<;
CJ
CS
2
s
o
2
2
c
2
m
fl*.
I
CD
3
to
UJ
z
CD
f-
o-
2222
3333
l'< ;y rf ;*<
O O O O
2222
^*
2222
3333
a o a c
"''22"°''
c in c o
in o-o
_i _i
- -
z
3
UJ
)•• •*"'
O
2
!*.-•
2
2
a
o
=
3
a
•^
^
i>
o-
2 2
3 3
c: a
2 2
2 2
? ?
C C
2 2
C O
r-i c-j
r;
_i
*
5 r
•--^ ^
_ .— .
— S
>• C.O
•> Cs
tz
2^
Z3
"Z
''C
^
Z;
«J
Ci-
>-
•_
^
j
CL
^
^r
-
^j
.
2
VM
B
'-i
215
-------
z,zzz z
I
_J -J -I -1.
til
13
a
=1
-1
in
zzzzzzzzz
oo
S
t- f- 1- t- H- U-
iiiiiiiiiiiiiiiiiiiigzzgiiiiiii'iiiiiiiiiiisiiiiiiii
UJ
t-
u>
— a
NUJ
UJ
cs
c
en
v-er.
ZUI
ziz1
1 §
ZZZZZZZZZZZZZZZZZZZZZZZZZZZZZZZZZZZZZZZZ
liillllllllilililiiillllllllillliilllllliilllllliiii
_ 2. z j:
Q
to
O'OOOOOliTOUTCfJIilOCCOOr-JOOOOC^OOg
OIJTOOOOOO
o o o o sj n w
MOOSO»CC3OOOOCSOlj~3GOOOOOOOU"3OOOp'O
W £j *"" X *"* N 2 § (^ £< in " r' ^ C° O § n O -rt J ^ ^ O rt 5 O O 111 llT PI O PI in PI PI O O O
CD *O O O *-i r+ r^ •& 111 m
rH P4 TI PI
z v-
-«
a
i
^t
*,
<-*
UJ
a
>«i
C£
O
_1
U
UJ
z
u
_l
>-
*™"
)—
UJ
-
i: x
a ui
c:r
0 -J
is: >-
CQ 1C
O t-
i: u
0 \
-J PJ
""• »^
Ci Ul
p-t »-4
a a
UJ
i- UJ
•c z
_J UJ
-
^"
a.
_•
>-
u.
O
a
!
2;
1
(-H
a
>-
X
)—
Ul
0
tt
0
_J
~
u
-c
Ci
r-
Ul
1-
LJ
^
UI
Zt
_I
o
1-
Ul
z
Ul
_]
>-
X
>-
UJ
5
o
f
x
CJ
hM
ii:
i-
— — cn co .
i i
C3 C2
x: z
^ CO —
LU _l CO
cn o a
- z:
rujM ziujzuj-j zi — —•-
o i. z = o ji ui i- _! a — a a u ,
cn a. •
co co
M D I
a co :
_i _j .
>- co
CO
>- UJ
' I- _5
•-H -^
ii z:
=. -
z
I C
Z UJ
- r:
P UJ
en uj
uj ~
~\ b-
C";
c <
-o co a CD -H « ^ rt -. n r-i n r-i r-i c-i n PI M
U.
U
£
t«4
^
Z
C
si
UJ _J
1- _J
UJ C
1— >-
C3 i-
' - '§
rJSrJnMWNNcJSwHMMPJWMMNNMCNNWNtMPlMNPJCVIplNPlPI, PI , C-l PI, PI PI fl PI PI PI PI PI P' Pi P! fi f-i C'J Q g
216
-------
i- i i T T -< T 7 T i i -i r-i .1 i T T
— ( 2 ^v LU ~
2 Q UJ >- 2 i
1 LU t-i _! _' LU X lu 2 oca:: _> '
1 • i. 22LULU S- M !— C3 _
lli O LU LU O Z3 ^ICi^UJ 2^
u. Lu'0-Ou.ii.O tU_IC! ^IU
iij' Ul 2-1 CEOO — LUOXS CLj
Z 2 LUZ OKCfOZCUO LUOi
^7 j; Da.otjir~2Si~p_i.j¥K
i ;5uia:^LCiCiCiC._iri>:cc:Et-cr-
f uj2.^-i 2 o_ 12
fi_ r-i r-j n M M fj i*i - r^ O1*
•«~t ^< ^H TH
1
'„ ^ ^0 - j - - ^ - :- 0 0
1 T-I -rt tH 1 « T 1 C i i O O -r-1 r-i T IS O O hi O rt O
2 . Z -.2 Z rt Z z 0 0 - CX-IMIT) 0 0
-< ' r-i rj Or-iOi=iCOO'.OOOO2O2OOOO
2 Z Z S3 ZZOO ^^*-~
_i 31 t X • LU ' ! ' •'"
Nl -J — i 2 LU Ce
uJ^J-KiujLuui-j rn:>- b T; r r
SoSijJ-xocc;orzn>-^LU>-zoLu2a(jiiuj~*_j
— i i rjccii— 01— -jCu^ci— cnucncc:L(_ r-i c N N is co co co' o o *H i-< TH »M v-c r-i r-i r-i r-i r-i r-i' r-i r-i
r-i r-i r-i r-i r-j r-i r-i r-i r-i r-i r-4 ri c-i r-i r-i r-i r-i r-i r-j r-i r^ r-i r-i r-i
rj r-i r-i r-i/c-j r-i r-j r-i rj-c-i r-j r-i r-i r-i r-i r-i c-i r-i r-i r.* rj r-i r-i c-j
ri n r-i n ri ri ri n.ri r-i r-J r-i r-i n r-i ri ri c-i r-i ci ri r-i r-i ri
-
•-0 M in T rs UT ^ rt rt rt CM
-J _!_•_!. _!_' _I _/-_! _l _I_1_I
22222222222222222222
= = = 3 = I3=ia = Z)=l=Z!OnS==* =
i ct" ii: Ci "LC ce ££ ii u: £c a: cs LE ti: C£ cs li ce ••". f,- '
liiiiiiiiii'iiiiiiiii
^^ CDs3rs>.u^rN>r%scoG^C"*i^io c- -o
rs rs. o^ 0s 0s co co r^ i-* cs &••
1
fs Q M .•
-o n n ^ >o _> _i .j is ii ~ !£ j £ ~ S ^ if. ;L
Cj — Q _J ^— I— !-- ^5 2 Q ' £ "'' ^ ~*- 1^ "^ ^~ '*" "'
zzco^-'Ooo- icci*xS-* I" ^
«a.uoi-i-H-i--uv.~
03 •;
r-i ^
......... .. .... c
r-i r-i n r-i r-i ri c-< ri CM r-i ri r-i r-i r-i r-i r-i r-i r-i ri n ^
r-i rj n ri ri r-i ri r-i n fi a ,-; n ri ri r-i r-i n ri ri
r-i CM ri ri c; r-i ri r-i r-i r-i n ri ri r-i r-i r-i n ri ri r.1 .r
)~
-
5
ti..
IX
<^'.
£
s.
~r
„
-
:.
— ,
-
-
~
_
i
^.
T
-
217
-------
o
r-i
i.
C
1
«
a
UJ
o
2
OOOOOOOOOOIXO^CNOCsOOOOOO
o o rs o* o* ON &*
o in o o o n o o o o. o o .o..o o
r-j ^t tn o T-( o o -^ ^o ro o o t-c o I
o -o o cs r-j -o n ii r -j
rt , r-J T ' V) llT
o o o o o
c o o n in
vj -
aa
i o
i _i_ cui
11-1X0
ZZ-J
>-iiiJ>-
^-uice
zc:uj
'-IICLJ
zoQ.
acea.
Htnt.-=Z3Dl-_ju— aciaji-i-i-i-i-_i>-3ii:
-UJUJMUiMZ:t-fii-KtJH"af—*— HJ—f— Z> H- ->
: o u
iS^
H Z U
n z z
1-1 UJ 3
tn i- a >-
uj i _i a z
z o c >• - o
:»• OJ
o
2
01
2
Q
M
1-
£J
- uj
i- _/
l-i £L
C£ Z
O «
1-1 tn
ce
a. >
2
i -
I Q
-J Z
cn
UJ c
i- >-
u zi
u
f-
A
ci r« rj rj ri <
pj M <••! rj rj i
i ri r-j c-i n ri rj r-i r-i ri r-i r-i n r-i r-i r-i r-i n r-i r-i r-i r-i ri n r-i r-i r-i n r-i n r-i r-i r-i r-i r-i r-i r-i n r-i r-i ri r-i r-i n r-i ri
I ri N rl r-J r-i r! r-i r-i r-i r-S rj r-; r-i r-i N r-i-N r-i r-i r-i c-i ri r-i M ri r-i r-i r-i r-i r-i r-i n r-i r-i r-i r-i « r-i r-i r-i n r-i r-i r-i r-i
Ui O
=; a.
o t-
2 -i
218
-------
UJ
«
3
a.
h-
LU
CD
*"j
cn
_
-s*5 iu
S^ J—
_l 0
H
1
1
1
1
U
1
1
1
1
C£
UJ
t—
UJ
I
•t
a.
a.
i
i
i
i
i
a.
CL
.
U
1^.
^
F*3 OGOOOa*HOOaa*-(ZZT-iP- -, i- H
O O ' ' Q O
z z z z
. -J -J -1 -1-1 -1 -I -i _J -I _J _J _1 _J _l
X
zzzzzzzzzzzzzzzzzzzzzzzzzzzz
3333333333333333333333333333
COGOOOOOOOOOO OOOOOOOOOOOOOOO
ZZZZZZZ2Z Z,Z ZZZZZZZZZZZZZZZZZ
,
"l
' «. •,-•••-
*r
• o-
zzzzzzzz z z zzozzzzzzzzzzzzzzz
333333333333^333333 33 3333333
lilCiliiCeiECtCiliiirCCiiCLi: £C. KCZCZiZiZCZCZKCZIZtZiZiZIZ
r— t— H ^-h— H-H-f— f— K- .&— h- h- h— ^- H- H- f— f— !— H- h- H-H-1—"- h-
OCjOOOOOOOOGO OOCOOOOCDOOOOOO O
ZZZ2ZZZ-Z-ZZZ:* ZZZZZZZZZZZZZZZ
; _i • , ' ' .
i
i-H i-l 1-1 C3 1 »-« i^ i-< ! W IM TH fx PI PJ *H O O PJ O M r-J TM O »H ^"
-I Z Z -rt PJ rt 0 0
" " -<:
Z ,Gi ' >- Z X -
ui o x a. i-
flj _l UJ I
o ui z: x -j a. uj
CC 2. U Uj' _J '- S
:C O LU UJ V. V. f.( _j ul UJ ' < - ' ' ^ *>
OXl-ZO-J H-lUt-UIZ > 3 'Z. 3Z:c 1-1
U.CJZUICiT UliIi3UI-UJZUi-<3:3 UI 3 3 i-iC3
O .>-!<£ _J O = _J 1 Ci-zxz3i-iuj>-3:ou.zci£Uj^_icj — a
_iPJ3f— oo-uicni— i i— uj-ji— cncccii^Lu-'3i-iZXOZ(j;UI-UJi--iCufll
u—u.a:i-iZu.a,aiCi- M
r*) ij"j Or *r T in u"t *o ^ co 03 *^ *o *r to TN Wi 0' o ••* rj T ij~ ^A r- ijo
M N w «r tn ii-j -o -o ^o -o N co Co n « -< T-I «. pi PJ M ti n f j tj PI
, :
• i-< ^ ^ U 0 NUrtpIrt
- •-_! -J _i _! _J _l _i _• _J _l
5^55gg55552:3zzzzzzzzzzzz
OOOOOOCOOOQCOOOOOOOCDOOOO
zzzzzzzzzzzzzzzzzzzzzzzz
- "'
zzzzzzzzzzzzzzzzzzzzzzzz
333333333333333333333333
ce &: u: o:Q;a:a:a;a;a:a:o;ii:c:a;fi:a;fi:fi:ci:a:a:a;££
t^^^.^^.^.^*_ ^^^.^-«_ .^<.^A_ ^M_^.^_
I v_. 1. ' ' . . «
•
^
o-OPJ orooocc-• n 13-
. -_j5'3 - -CCCi^
acj_ji-!-!-i-i-_'i-3i:oz_J3i:a_iZr-z'-a
coiHooooooo_j-h-r>>-<:aii-iEui:oiCJ3:t-i-^>-(n
ul
!— '
C
Z
LU
Ci
. -
2
^
<2
r~
9
S
M*
' t_
C^
u.
ID a
« iil
S b
' 3: •-* •
_j
C C
!— S
Ij J-U
C'-'I
u.
>- LiJ
•—f ;!_
^ -
0 i-
Z 1-1
M r-j r-j r-i r-i r-j r-j r-j
I PI M n PI PI PJ PI PI Pi H n -j « W PJ PI pi P! w PI rj pi PI pi r-i c, c; PI PI rlri P! P! S P! P! S PJ S P; S • a 5
219
-------
-------
APPENDIX I
TABULATIONS OF ANSWERS TO SELECTED QUESTIONS
FROM THE DATA COLLECTION PORTFOLIO
(Refer to Appendix A)
221
-------
-------
03/21/78
FILE - INK
- CREATED 03/21/78
1
DFl ATTW
... ' , ABSOLUTE FREQ
CATEGORY LA8EL , COpE FREQ (PCT)
AL
A°
. •" - ; -*z>/ _
CA;
CO
CT
DC
FL
GA
1 .. , , - .' . Hi
— • • ' • IA
IL
•..:'• IN: _' .
' KC'
KY:
LA
i . . ' .
i " .*•--!•'
' " * MA
> ' "
- • . MO;
,M1.
: !
MM
, MO
• ' • - •
- : MS'
' ' Mr
2
2
4
47
5
6
1
14'
20
2
3
46
7
?
4
9
•5*
£. 1-
9
13
16
i
10
0.4
0.4
0.9
10.2
1*1
1.3
0.2
3 . n
4,3
/
0.4
n j.7
10,0
1.5
I
ft ^
0«9
- 2.0
4/L
•eO
2.0
R.a
.0
3.5
0.2
2.2
E A43JUS-T?
FREQ
(PCT)
0.4
0.4
0.9
10.2
i _, i
1.3
0.2
3.0
4.3
0.4"
ft 7
10.0
1.5
ao
0.9
' 2.0
4.6
2.0
2.8
2.0
'"i
.3.5
0.2
2.2
"n n IM
FREQ
(PCT)
0.4
O.Q
1.7
12.0
i •» n
14.3
14.6
1 7 A •
, i-f-»-<3
22.0
22.4
\ '
5T ft
— -&J t-V—
33.0
'-/. " »
34.6
4fl
3S'.7
37.6
42.2 -
44.1 " ,
47.0
48.9
,52.4
52.6
' 54.8
223
-------
03/22/76
FILE - iNK
- CKtATEO 03/22/78
HAOt 21
0.4
0.4
55.2
NH
0.4
0.4
NY
34
7.4
7.4
5S.7
7:L.b
OH
28
-Q*r-
6,1
-G-.-2-
OR
1.5
6.1
-Q-r2-
1.5
77.6
-Wv6-
79.3
PA
24
5.2
-R-t-
SC
-G-r2-
0.7
5.2
-O-i-2-
0.7
84.6
-B4-.-Q-
d5.^
TN
-T*-
UT
13
-2-2-
3
2.8
-^4-r8-
0.7
2.8
-4-rS-
0.7
BQ.3
93.7
VA
2.0
-V?AT
WI
TOTAL
14
• *••§'*•' »••*!
460
1—3-
3.0
100.0
2.0
t-rf-
3.0
- «1»-»'^»-*w-«
100.0
95.7
100.0
VALID CASES
460
MISSING CASES
224
-------
QS
TYPE OF BUSINESS ORGANIZATION
CATEGORY LABEL
PUBLIC CORP
-PJ5.1VATE_.C.ORP-. _
PARTNERSHIP
PROPRIETORS
-COOPERATIVE
CODE
ABSOLUTE
FREQ
193
RELATIVE ADJUSTED
FREQ
(PCT)
42.0
FREQ
(PCT)
42.3
CUM-
FREQ
(PCT)
42.3
P C
SHIP D
P - ''• -• P s
' 6
9
T
1.3
2.0
0,2
1.3
2.0
0.2
97.8
99.8
100 0
TOTAL
4 0.9 MISSING 100.0
460 100.0 100.0
VALID CASES
456
MISSING CASES
225
-------
03/21/78
.DA-
- INK
- CREATED 03/21/78
CTATIIC nr TMC- 0
L-AMI_&I4CE-
CATEGORY LABEL
5NLY SITE
BRANCH PLA.N|T-
DIVISION
CAPTIVE SITE
VALID CASES 454
.
CODE
A
p. -
c
D
TOTaL
MISSING
'" f
ABSOLUTE
FREQ
128
26 /
7
1 •
460
CASES 6
5ELA-T.-I-V-E-
FREQ
(PCT)
27.8
63.7
5.7
1.5
1^3
100.0
—ADJUSTED
FREQ
(PCT)
28.2
5«7
1.5
MTSSTNG
ioo.o
CUM
FREQ
(PCT)
28.2
92' j,7
98.5
100.0
1 nri n
• • •
RELATIVE
ABSOLUTE FREQ
CATEGORY LABEL CODE FREQ (PCT)
COST CENTER A 22 4.8.
I
PROFTT TFNTFP B ?Q7 A4.A
141 30.7
TOTAL 460 , 100.0
VALID CASES 319 MISSING CASES 141
ADJUSTED
FREQ
(PCT)
609
MISSING
100. 0
•
CUM
FREQ
(PCT)
6.9
1 no o
.100.0
226
-------
03/21/78
FILE - INK
- CREATED 03/21/78
f • , ; ••
CATEGORY LABEL
LESS THAN ''10
in Tn ?n
21 TO 30
31 TO 40 ' " ,
A! rn PQ
51 TO 60
61 TO 70
71 TO-80
81 TO 90
I 91 TO 100 ;
^ ini jn i"e;n
OVER ISO
— VALID CASES '- . i 458 -
)
CODE
""' A ;
H
C '
0
E
F
G
H
I
J
K
L
X >
TOTM
MISSING
- ;
f
ABSOLUTE
FREQ
195
133
59 '
26
14
3
5
3
4
3
9
4
. . . . 2
/,An
CASES -. 2
?ELAXIVE — AOJUSIEO-
FREQ FREQ
(PCT) (PCT)
42.4
JB.Q
12.8
5.7
3.0
0.7
i . i
A 7
,0.9
0.7
2 b
0.9
P.-*
T Art n
42.6
2°. 0
12.9
5.7
3* i
0.7
1.1
07
0.9
0.7
2 0
0.9
MISSING
i An n
i-U-W- «-U
/
CUM
FREO
-------
I 03/21/78
FILE - INK
- CREATED 03/21/78
Q9
MAXIMUM 1976 EMPLOYMENT
CATEGORY LABEL
LESS THAN 10
1Q TO 20
RELATIVE—ADJUSTED-
ABSOLUTE FREQ FREQ.
CODE FREQ (PCT) CPCT3
_-.CUM.-
FREQ
(PCT)
A
_B_
178
38.7
21 Tp 30
~31 TO 40
_A1_T.O_50-
C
D
59
29
12.8
"'6.3
40.3
-29,4-
13.3
'6.6
40.3
69.7
83.0
89.6
92>,5,
51 TO 60
61 TO 70
71 Tn an
F
G
6
4
1.3
0.9
1,4
"0.9
93.9
94.8
95,2
81 TO 90
.0.9
0.9
96.2
91 TO 100
0.9
0.9
97.1
i ni Tr\ i c;n
OVER 150
K
L
Q
4
^ fl
0.9
?.;()
0.9
00 i
100.0
^10141=-
.18
mf»*mi**
-A60-
-VALLD CASES
MISSING-CASE*
3.9
4^0-^0-
-18
MISSING
i04J^-0-
100.0
228
-------
[
'
03/21/78 :, FII
Q10 AGE-OF PL At
CATEGORY LABEL
LESS THAN, 3
3 TO c;
6 TO 10
11 TO 20
OVER 30 YEARS
• •
1- — UAL-I.D. CASES ,-448 .
i •
Gil-.-— TOTAL 1976
CATEGORY LABEL
UNDER 200000 LSS'
_2_o.oooo TO SfiQnnq
500K TO 1MM
1MM TO 3MM
O.VER -3-MTM..ION—
—
•
_E - INK - CREATED
MT
• . i • -
ABSOLUTE
CQOE FREQ
A 49
B e?l
C : 98
0 126
E 60
F 64
12
TOTAL 460
- - MISSING CASES 1-Z
VOLUME IN POUNDc
: ABSOLUTE
CODE FREQ
. A 1.21"
R • 76
C . 79
D "" 75
P ' 69
40
TOTAL 460
03/21/78
_J3PI ATT UP
FREQ
(PCT)
10.7
11,1
21.3
27.4
1 "5, ft
13.9
2.6
inn r»
-RELATIVE -
FREQ
(PCT)
26.3
16.5
17.2
16.3
8-7
100.0
-AOJUSIE-D—
FREQ
(PCT>
10.9
1 1 -ti.
21.9
28.1
i ^ ti.
14.3
MISSING
i t\f\ n
-
FREQ
(PCT)
28.8
18,- 1
18.8
17.9
16.4
MISSING
100.0
-.
FREQ
(PCT)-
10.9
44.2
72.3
100.0
100..0
/^f tlut
FRFQ
(PCT)
28.8
46 Q
65.7
83.6
i r>n rt
100.0
'--
VALID CASES
420
MISSING CASES
40
229
-------
03/21/78 FILE -
?
CATEGORY LABEL
0' TO 10
1 i Tn pri
21 TO 30
31 TO 40
A'I Tn i^n
51 TO 60
61 TO 70
71" TO an
ai TO 90
91 TO 100
VALID CASES 398
V Q14 AVERAGE ANNUAL
CATEGORY LABEL
UNDER 200000 LBS,
gjJOUOll IJJ — DU.UUJJU. _
500K fO 1MM
IMM TO 3MM
rn/crn -a UTI I TOM
1
INK - CREATED
ABSOLUTE
C05E FREQ
A 5
R 1<3
C 26
D 77'
E ^°
F 46
G 59
H 48
I' 30
J 29
TOTAL 460
03/21/78
FREQ
(PCT)
1.1
A.T
5.7
16.7
1-2.8
10.0
12.8
' 6.5
6.3
ioo.o
_
FREQ
(PCT)
1.3
4.8
6.5
19.3
14^,3 . -
11.6
I40a
7.5
7.3
—M4-SS5-NG—
ioo.o
CUM
FREQ
(PCT)
1.3
6,0 -
12.6
31.9
/,<;, 7
58.3
73.1
85.2
92.7
100.0
-WO.-0 ,
MISSING CASES 62 .
PRODUCTION
ABSOLUTE
CODE FREQ
A 124-
C 68
D 59
F &.\-
61
TOTAL 460
. RELATIVE.
FREQ
27.0
14.8
12.8
1 ** . "»-
13.3
100.0
-^ADJUSTED-
FREQ
(PCT)
31.1
17.0
14.8
15.3
MISSING
ioo.o
CUM
FREQ
(PCT)
31 „ 1
52^.9,, •
69.9
84.7
1.00.0
100.0
•
VALID CASES
399
MISSING CASES
230
-------
03/21/78
FILE - INK
- CREATED 03/21/78
CATEGORY LABEL
LESS THAN 250K
500K TO 750K
75, OK TO 1~MM
IMM TO 1.25MM
1.25MM TO 1.5MM
1.5 TO 3MM
i
VALID CASES 372
-•• -017- - NUMBER OF
i
CATEGORY LA8EL '
ONE SHIFT
T.WQ_SHIE±S. . : .
THREE SHIFTS
1
sJ-fG. — -WP r*KwLJUlr.
C05E
A
B
c ;
D ,
E
F
G
H '
"TOTAL
MISSING
1 iUN
ABSOLUTE
FREO
85
76 '
40
31
35
49
42
a?
460
CASES 88
SHIFTS PER DAY
CODE
A
._.._.'• a
C
ZOlAL
'ABSOLUTE
FREO
373
73
13
'. .-. 1
AArt
Dpi ATT\/I
FREQ
-------
03/21/78
FILE - INK
- CREATED 03/21/78
nr CMTFTC
ABSOLUTE
CATEGORY LABEL CODE" FREQ
7 HOURS A 7
fl* R &T^
10 • C 7
12 0 1
13
TOTAL 460
VALID CASES 447 MISSING CASES 13
*N-*« in uiQC-n nc- n A Vff oiro utre'V
FREQ FREQ
(PCT) (PCT)
1.5 1.6
1.5' 1.6
0.2 0.2
2.8 MISSING
100.0 100.0
FREQ
(PCT)
1.6
99.8
100.0
ioo.o -
t
CATEGORY LABEL CODE
LESS THAN 4- A
6 D
TOTAL
ABSOLUTE
FREQ
10
6
460
(PCT)
FREQ
(PCT)
FRFQ
(PCT)
2.2
2.2
2.2
93.7
1.3
100.0
1.3
100.0
100.0
VALID CASES
'460
MISSING CASES
232
-------
03/21/78
FJLE - INK
-CREATED 03/21/78
> 021 NUMBER OF, TUBS LESS THAN 5 GALS
• ; .• ,
CATEGORY LABEL CODE
0 A
L_TQ 5 __... ' . . p
6 TO 1 0 C
10 TO 20 D
20 TO =;n p
OVER 50 F
' - ' ' - ' «•»•
VALID. CASES 300 .-MISSIMG
.
^ °^2 TUBS 6 TO 10 GALS
.CATEGORY LABEL CODE
: 0 A
6 TO 10 C
10 TO 20 ' D
OVER 50 F
' TOTAL-
VALID CASES 276 . --MISSING.,,
• ABSOLUTE
, FREQ
123
72
45
; 46
Q
5.
T Jp.o "
4Af)
_
p
ABSOLUTE
FREQ
';. 123
AC; . •
45
31
7
5
: 184
. 460
CASES 134.
RELATIV
FREQ
(PCT)
26.7
9.8
10.6
2« 0
1.1
34,8
100.0
^>-
FREQ
(PCT)
26.7
14.1
9,8
6.7
1 S
1.1
40.0
On
'P AD IIICTPn
FREQ
(PCT)
41.6
74 n
15.0
15.3 ,
1.7
MISSING
100.0
EX n ii icTpn
FREQ
(PCT)
44.6
, 16.3
11.2
•3
-------
03/21/78 FILE - INK - CREATED 03/21/78
S Q23 TUBS 10 TO r>0 GALS
[ PPLATJVP iDJUSTFO-
ABSOLUTE FREQ' FREQ .
CATEGORY LABEL CODE FREO (PCT) (PCT)
0*™ A 41 8.9 11. 1
i TO * R no ?^-o •*?•,:*
6 to .10 C 94 20.4 25.4
10 TO 20 0 78 17.6 21.1
9n Tn =;n F ^n £.5 fl.l
OVER 50 F 8 1.7 2.2
| .90 .19.6 MISSING
Tn'f AL 4Aft io^.O 100.0
Ufti Tn r&c;Ft; 370 MTC^TWR CA^F*;' Q(j
I -
qg|_/\T^yp ^n lllgTCTL
• ABSOLUTE FREQ FREQ.
CATEGORY LABEL COnE FREO (PCT) (PCT)
0 A 54 11.7 15.9
6 TO 10 C 96 20.9 28.3
10 to 20 D 61 13.3 18.0
•an Tn Cn f 1 7 "* . 7 e;— Q
OVER 50 F 4 0.9 1.2
121 26.3 MISSING
TOTJM 46
-------
Q3/E1/73 FILE - INK - CREATED 03/21/78
V- 025 TUBS 101 TO 250 GALS
, , -
v- .- ABSOLUTE
, CATEGORY LABEL CODE FREQ
0 ~~~~ ' . - . .". A ; ~\ us
6 TO 10 .< \ C i 45
; 10 TO 20 o 20
2Q_TO_«5n F • 10
. ; -163
TOTAL 460
RELATIVE
FREQ
(PCT)
25.7
9.8
4.3
35.4
100.0 ,,
— AOJUSTEO-
FREQ
(PCT)
39,7~~
15.2
6.7
1 A.
MISSING
100.0
FREQ
(PCT)
39.7
7 A .7
89.9
96.6
100. 0
VALID 'CASES 297 MISSING CASES .163
s — -Q?A ™8S 2^1 TO 500 GALS
\ • l
: PFI ATT\/P
ABSOLUTE FREQ -
CATEGORY .LABEL _ CODE FREQ (PCT)
0 A . r 162
i TO q R c,,
6 TO '10 C 12
10 TO 20 D 11
OVER 50 F 2
' - :- .".' ' : 213
-— - TOTAL 460
VALID CASES. ..247. MISSIMG CASFS 213
35.2
i T -. i
2.6
2.4
.0.4
46.3
ijin n
AH n icTtrn
FREQ
(PCT)
65.6
PI- q
4.9
2 4
• ,0.8
MISSING
inn ft
M.
FREQ
(PCT)
65.6
07 /,
92.3
96.8
QQ ?
1 0-0 .0
100.0
V • . ' ' . -
235 '
-------
03/21/78
FILE - INK
- CREATED 03/21/78
J>. UHf,_ _.,- 1 UDO 3Ui IU 1UUU <3HUS
RELATIVE-. ADJUSTED-
ABSOLUTE FREQ FREQ
CATFGORY LABEL CODE FREQ (PCT) (PCT)
'0 A 188 40.9 83.6
1 TO <=; R ?7 ^T<3 1?Tn
6 TO 10 C 4 0.9 i.8
' 10 TO 20 D 6 1.3 2.7
2-^ *i.l MlsqTNfl __
TOTAL 460 100.0 100.0
VALID CASES 225 MISSING CASES 235
,
r L
PFLAT-1-«F ATLUJ«3iEn_
ABSOLUTE FREQ FREQ
CATEGORY LABEL CODE FREQ (PCT) (PCT)
0 A 195 42.4 92.0
1 TO
-------
03/21/78 : FILE - INK - CREATED 03/21/78
">- 029 NUMBER OF 'PRODUCTION : DAYS PER YEAR
_ — ..... .. .'. .. , .„ ..--. ._...._,.;.. -. •-.„_..-, ,-.„.„. DPI ATTVC
CATEGORY LABEL
150 to 200~
??ni TO 25.0
251 TO 300
301 TO 365
UNDFR Tqn
VALID CASES
ABSOLUTE FREQ
CODE FREQ (PCT)
A 13
R 21°
C , 204
' , D "• ' 17
F- -a*
;, s ,
TOTAL 460
455 MISSING CASES 5
2.3
44.3
3.7
0*4
.1-1
100. 0
*n JUSTFn
FREQ
(PCT)
2.9
44.8
3.7
0.4
MISSING
100.0
CUM
FREQ
(PCT)
2.9
•51 0
95.8
99.6
inn n
100. 0
> Q31 ...'-. . GALS
CATEGORY LABEL
0 TO 10000
1.0.0 0.0. TJO_.2_Q.Q.QCL
20000 TO 30000
' 30000 to 50000
__50K T0_l DDK.
^ VALID CASES
OF WATER USED FOR ALL PURPOSES
• • R
. i ABSOLUTE
' CODE FREQ
A ' 376
R - 32 . '
C 13
.0 • &•
...-'• 27
TOTAL 460
433 MISSING CASES 27
ELATIVE A-DJUSIEO-
FREQ FREQ
(PCT) (PCT)
81.7
7,0
2,3
1.3
i .3
5.. 9
100.0
86.8
7»4
3.0
1.4
1 .4
MISSING
100.0
•
FPEQ
(PCT)
86.8
97.2
98.6
i nn n
100.0 ,
-. -
237
-------
03/21/78 FILE - INK - CREATED 03/21/78
^ rpT ocorc-MT ne- uXrpp nSFn TM PRODUCT
RELATIVE
ABSOLUTE FREQ
CATEGORY LABEL ; CODE FREQ (PCT)
0 A 201 43.7
| Tn i-ii R \*\ i^t^
11 TO- 20 C 24 5.2
21 TO 30 08 1.7
•31 Tn 4n P ig 3*9
41 TO §6 F '6 1.3
51 TO 60 G 1 0.2
fl TO 70 H 3 0,7
71 TO 80 I 5' ,1.1
81 TO 90 J 4 6.9
°1 TO °9 K '3 6m7
100 LI 0.2
35 7.6
TOTaL 460 100 6
VALID CASES • 42^ MISSIMG CASES 35
-
-
ADJUS^gO—
FREQ
(PCT)
47.3
3^ a 5
5.6
1.9
L. -S
i.4
0.2
0 ,7
1.2
0,9
0*7
0.2
MISSING
100..0
/
,,, CUM „ ' .'
FRFQ
-------
J 03/21/78 • FILE - INK ; - CREATED 03/21/78
f" y
> '034-.-.-. ... PERCENT Or WATER FOR COOLIMG
~ RFI ATTVF
• ' ' ; ABSOLUTE FREQ -
CATEGORY LABEL CODE FREQ (PCT)
0 A 42 9.1
1 TO 10 R , . 5-3 11,5
11 TO 20 - - . . C . '38 8.3
21 TO 30 D 29 6.3
_1. .31 TO 40 P •'?*'• *,7
41 TO 50 F 26 5.7
51 TO 60 G ; 24 5.2
f>\ tn 7p H 27 5 o
71 TO 80 I 35 7.6
81 TO 90 J 70 _ 15.2
•31 Tn oa «• , A* 14.3
100 L 5 1.1
' : .19 f-.l
TOTAL 460 inn n
; .-. ,, ,'.,.,, \
•• ' ' : '
1 s'
1 •
AD-JUSTED CUM
FREQ - FREQ
(PCT)
-------
03/21/78 FILE
> 035 DFC"'*FK!T ^F Wy
i
i
CATEGORY LABEL
6
1 Jn in
11 TO 20
21 TO 30
31 TO 40
41 TO SO
51 TO 60
01 Tn Qrj
-INK - CREATED
TER FOP BnILEP FEED
CODE
A
C
D
F
G
j
TOTAL
ABSOLUTE
FREQ
229
11
3
2
1 -
75
460
VALID CASES 385 MISSING CAS^S 7
^ ..Q36 ... PERCENT OF WATER FOR TUB CLEANING
i
CATEGORY LABEL
0
1 TO i n
11 TO 20
21 TO 30
**i Tn in
, JJ_LQ_*D
41 T.O 50
VALSD CASES ...399
CODE
A
R
C
D
P
F
TOT.AI ,_
MISS IMG.
ABSOLUTE
FREQ
179
IfiT
30
11
7
5
61
iftn
03/21/78
RELATIVE
FREQ
-------
03/21/78
FILE - INK
- CREATED 03/21/78
f ' ;.••' :• — '; ' .
"ELATIVE ADJUSTED CUM
i - . -. . . ABSOLUTE FREQ FREQ " FREQ
CATEGORY LABEL CODE FREQ (PCT) (PCT> (PCT)
0 A 20 4.3
1 T° lfl fl ' IBI' 1Q.3
11 TO 20 C 64 13.9
1 21 TO 30 ; 6 - 19 4.1
7T TO in . . E ' 21 4.6
41 TO 50 F 49 10.7
51 TO 60 , G 24 5.2
61 TO 70 H 11 2*4
71 TO 80 , I / 1-3 - 2.8
81 TO 90 , J 6 i.3
i
°1 TO °9 K 11 2,4
100 L ' 8 1.7
• 33. 7.2
TOTAL 460 1 00 0
i r
VALID- CASES 427 MISSIMG CASES 33
i
4.7 4.7
15.0 62.1
4.4 66.5
i..a 71 i*.
11.5 82.9
5.6 88.5
2^6 91'
3.0 94.1
1.4 95.6
?,A an \
1.9 100.0
MISSING 100.0
Too o
••- • • ; • "
• . " ! '.'"--
' •'
: -- ••- - - - - -• - -'
. 241
-------
03/21/78 FILE - INK - CREATED 03/21/78
> Q38 . PERCENT OF WATER FOR AIR POLLUTION CONTR
RFI ATTVE...
CATEGORY LABEL
6
1 TO VO
61 TO 70
91 TO 99
VALID' CASES 353
CODE
A
H
H
K
TOTAL
MISSING
'ABSOLUTE FRE^.
FREQ (PCT)
344 , 7t.8
'• i»*
1 6.2
1 6.2
1 Q"r' 7."*\ •» - - -
460 100.0
CASES' lOT
-ADJUSTED-
FREQ.
(PCT)
97. S
?,Q
0.3
6.3
...MISS-ING- ...
100.0
... CUM
FREQ
(PCT)
97.5
QP.4.
99.7
100.0
100 0
.
n-JO OFDfTMT HP"
CATEGORY LABEL
0
i TO i n
11 TO 20
21 TO 30
ai Tn Qn
91 TO 99
VAI Tn rA«?F«;. .. 256
WATEP FOR OTutrD o'looncre
conE
A
p
c
D
j
K
f nfj\L
MISSING
OEL'TT-"*7
ABSOLUTE FREQ
FREQ (PCT)
237 51.5
i? ?.*
3 0.7
2 -0.4
7 " (} t' p
1 . 0.2
204 44.3
460 In6,0
CASES ... 204
ADJUSTED-
FREQ
(PCT)
92.6
4.7
1.2
0.8
0,4
0.4
MISSING
ioo,o -
1
CUM
FREQ
(PCT) ,
92.6
97^3
98.4
99,2
....99.6
100.0
1 00 . 0
242
-------
03/21/76 ; FILE— INK
- CREATED 03/21/78
v ._Q4Q. GFMFRAl ^AI F^
[
- •• ABSOLUTE
CATEGORY LABEL " CODE. FREQ
6 A ; n
1-iO .10 R '- IA
11 TO 20 . c ' 5
21 TO 30 0 2
41 TO 50 - F 3
—51 TO- 60 G £
6.1 tn 7n u ! a
71 TO 80 I 14,
81 TO 90 j 22
— 9l_io_9P K ;,n
iOO L 298
. 36 ..
• TOT^t 460
\
—VALID-CASES 4E4 MISSING CASES 36
RELATIVE
FREQ
(PCT)
2.A
T,<7
1.1
0.4
6 ,Q
0.7
0.4
9. n
4.8
fl-7'
64.8
7.8
fnn A
An HicTcn /•! iu
FREQ FREQ
(PCTJ (PCT)
2.6 2.6
T-T ^:~Q
J.-3 ~ . ^
1.2 7.1.
0.5 7.5
no Q c
0.7 9.2
0.5 9.7
"?' 1 V 1 a
: C^-i 1 I .8
3.3 15.1
5.2 20.3
9L -3Q t
70.3 100..0
MISSING ,100.0
i n n n
.
''- •
[ : X
I - - '
•••'.;
x .
\
243
-------
03/21/78 FILE - INK - CREATED 03/21/78
<. OM rA.PTTVF PPQOi"*TTON
OEL'VTT/E ADJ'JSTED
ABSOLUTE FREQ FREQ
CAJEGORY LABEL CODE FREQ (PCT (PCT)
0 A 302 65.7 73.8
\ rn jn p ^4 7.4. R,T
11 TO 20 C 22 4.8 5.4
21 TO 30 0 11 2.4 2.7
41 TO 50 F 3 0.7 0.7
51 TO 60 G 3 0.7 0.7
M Tn 7n H 3 0»7 n.7
71 TO 80 I 4 0.9 1.0
81 TO 90 J 4- 6.9 1.0
ejj yn oa K 7 1»5 1»7
100 L 8 1.7 2.0
51 11.1 M.ISSING
TOTAL 460 100 0 100 0
VALID CASES 409 MISSING CASFS "51 •- - - -
CUM
FREQ
-------
03/21/78
FILE - INK
- CREATED 03/21/73
.-042 .. PASTE INK PRODUCTION
. . , ABSOLUTE
CATEGORY LABEL CODE FREQ
0 A 60
i" to in R ii
11 TO 20 C i 27
21 TO 30 D 20
31 TO 4n F. j'q
41 TO 50 F 44
51 TO 60 6 15
].. 61 Tn 7n ' H ' . - i-j
. 71 TO 80 I 14
81 TO 90 J 16
100 - L :• • • 178
- •: ' . " .9
TOTAL 460
VAI LD CASF;^ • &*l M ISSXWG— CASES
•' ' !
RELATIVE
FREQ
(PCT)
13.0
2.4
5.9
4.3
9.6
3.3
2. a
3.6
3.5
fl^T
38.7
2»P
1 00 * 0
Q
>
ADJUSTED
FREQ
-------
03/21/78
w nA-» LTO^in
s*
\
CATEGORY LABEL
0
i TO in
11 TO 20 -
21 TO 30
T| Tf) iQ
41 TO 50
51 TO 60
f>\ T° 70
71 TO-30-
81 TO 90
ni Tn QQ_
00
i
VAI TH f^AcrF'^
1
f
FILE - INK - CREATED
JKJI^ p(?OD(,irf IOM
ABSOLUTE
CODE FREQ
A 180
R 37
C 14
D 13
p- i?
F 30
G 33
H 15'
I 22
J 20
K 10
L 56
18
TOTil 460
AAP' MT^STMG CASES 1
'
03/21/78
•RELAT-IVE ADJUSTED-
FREQ FREQ
(PCT) (PCT)
39»1 40.7
p,n n,A
3,0 3.2
2'.8 2.9
2; 6 2.7
6.5 6,8
7.2 7.5
3.3 "**4
4.8 5,0
4.3 4.5
2 2 2.3
12.2 12.7
3.9 MISSING
looo iooo
3 , , ,
\
\
\
FREQ
(PCT3
40.7
49.1 - ~^-
52.3
55.2
6407
7202
7S „ 6 -
80.5
85.1
87^3
100.0
ioo.6
246
-------
03/21/78
FILE - INK
- CREATED 03/21/78
Q44.... ...... WATER BASE INK PRODUCTION
_ _..: — — . . _.. . ___ : _ .RELATIVE
- . : ABSOLUTE FREQ
CATEGORY LABEL CODE FREQ
-------
03/21/78
FILE - INK
- CREATED 03/21/78
^ 'W? - 1 L ~."i*~ JIN". h"^'."'L"- ' l'j'"i
PPI ATTVP An.in
-------
FILE - INK
-CREATED 03/21/78
^..046...
SOLVENT BASE INK PRODUCTION
I
. ......
CATEGORY LABEL
1 Td 10
11 TO 20
21 TO 30
_ _3.1_IQ 40
j 41 TO 50
51 TO 60
( 61 Tr> 70
71 TO 80
L_. _.._
81 TO 90
, <31 rn QQ
100
-VALID. CASES .-_ 437
.. ... ... . *_^.,.^.. •• RELATIVE-. -ADJUSTED -
ABSOLUTE FREQ FRPQ
CODE FREQ (PCT) (PCT)
A 221 48.0 50.6
R ' "*? 7,0 7 j
C 15 3.3 3.4
0 19 4.1 4.3
£ 21 A A A Q
F 46 10.0 10.5
G 12 2.6 2.7
H 11 _? A 5 C
I 11 2.4 2.5
J 14 3-0 3.2
K IT p. ft in
L 22 4.8 5.0
?3 5.0 MISSING
TOTA*' A£,n inn rt irtA rt
— .. MISSING_CASE!5 ?^
\
••
- CUM
FREQ
(PCT)
50.6
= 7 q
61.3
65.7
"7 n c
7.0-..5-
81.0
83.8
Q JC *3
. 88.8
92.0
QC ft
100.0
100.0
- '
:
249
-------
03/21/78
FILE - INK
- CREATED 03/21/78
w n/. *y nortAMTPOT CMPMTC » tern
•
PFL*TTUP
ABSOLUTE FREO
CATEGORY LABEL CODE FREQ (PCT)
6 A 19 4.1
i rn in n ?^ 5.7
11 TO 20 C 30 6.5
21 TO 30 D 26 5.7
11 TO 40 E 23" c^0
41 TO 50 F / 69 15.0
51 TO 60 G 17 3.7
A1 TH TO U "3C 5 4
71 TO 80 ,1 34 , 7.4
81 TO 90 J 35 7.6
oV Tn QQ K 99 21.5
100 L 29 6.3
28 6.1
TAT * i 46A Tonn
\/ Al T n P ACtTC A*7C3 MtCCTMfi PAQ?"^ ?fl
1
f
ADJUST-SO—
FREQ
(PCT)
4.4
6.0
6.9
6.0
16.0
3.9
5V8
7.9
8.1
22*9
6.7
MISSING
100 0
i^UM
FREQ
(PCT)
4.4
17.4
23.4
...2 8 .7 -
44,7
48 „ 6
54U4 • :.
62.3
70.4
—-93.3
100.0
100.0
. .. .•__
250
-------
I 03/21/73 FILE - INK" , - CREATED 03/21/78
046 INORGANIC PIGMENT. USAGE
CATEGORY LABEL
0
1 TO 10
11 TO 20
21 TO 30
31 TO 4n
41 TO 50
51 TO 60
61 Tn 7n
71 TO 80
1
81 TO 90
-------
I.
03/21/78 FILE - INK
-Q50 ._.. WATER RINSE OF TUBS
- CREATED 03/21/78
CATEGORY LABEL
"YES
,..-- RELATIVE-ADJUSTED OJM_
ABSOLUTE FREQ FREQ FRF.Q
CODE FREQ (PCT) (PCT) (PCT)
A
TOTAL
158
-,n?
460
34.3
6=;. 7
100.0
100.0 ,
HjcjqjNrt
100.0
100.0
1 Ona n
VALID CASES
158
MISSING CASES 302
oci
r/utcTTr UACU ne- Tune
"E'LATIVE ADJUSTED CUM
ABSOLUTE FREQ FREQ FREQ
CATEGORY LABEL CODE FREQ (PCT) (PCT) (PCT)
YES B 111
•340
24.1
7^.9
100.0 100.0
~
TOTAL 460
100.0
100.0
VALID CASES 111 MISSING CASES 349
• '
>-
0,52.,,
SOLVENT WASH OF TUBS
CATEGORY LABEL
YES "
. RELATIVE .. ADJUSTED--
ABSOLUTE FREQ FREQ
CODE FREQ (PCT) (PCT) (PCT)
TOTAL
308 ' 67.0 100.0 100.0
-152 33.0 _, MISS ING 1.00.0.
460 100.0 100.0
VALID CASES
308
MISSING CASES 152
252
-------
03/21/78
FILE - IN*
- CREATED 03/21/78
PC;-3
f
CATEGORY LABEL
YES
VALID CASES 106
v_ Q54 PERIODIC CA
CATEGORY LABEL
YES
VALID CASES 85
, D
ABSOLUTE
COOE FREO
D 106
i . •
TOTAL 460
i .
MISSING CASES 354
USTIC SOAKING
R
ABSOLUTE
CODE \ FREQ
E ; 85
• - - . 375
TOTAL 460
MISSING CASES 375
ELAT-I-VE—
FREQ
(PCT)
23.0
77.0
100.0
ELATIVE—
FREQ
(PCT)
18.5
ai .=;
ioo.o
AOJUST-ED
FREQ
(PCT)
100.0
MISSING
100.0
ADJUSTED
FREQ
(PCT)
ioo.o
MISSING
100.0
CUM
FREQ
(PCT)
ioo.o
100.0
CUM
FRFQ
(PCT)
100.0 .
100. «
v. — CL=L<^ TYP'1' nr C/11
CATEGORY LA8EL
CLOSED LOOP
OPFN
PARTIAL RECYCLE
VALID-CASES ,_173.
JSTI'* WASHING SYSTEM
ABSOLUTE
CODE FREQ
A 68
C : , 25
i 287
TOTAL 460
... MISS-LMG-JCASES - g87
i 253
M<;cn
FREQ
(PCT)
14.8
17.4
5,4
62.4
100 n
ADJUSTED
FREQ
(PCT)
39.3
4.A ?
14,5
MISSING
i nn n
Pt IM
FREQ
(PCT)
39.3
100.0
100.0
-------
03/21/78
FILE - INK
- CREATED 03/21/78
— WATER PRESSURE USED FOR WATER WASH
i
I
CATEGORY LABEL
LESS THAN 50 PSI
51 TO TOO PST
101 TO 150 PSI
OVER 150 PSI
VALID CASES 196
CATEGORY LABEL
ALL OF THE TIME
Mr>e;T DP" TWF TTMF
OCCASSIONALLY
NEVER
VALID CASES 444
i
PFI ATTVF Xn II ICTPn
ABSOLUTE FREQ FREQ
CODE FREQ (PCT) (PCT)
A 149 32.4 76.0
R 4=; Q.R ?"*,0
C 1 0.2 0.5
D 1 0.2 0.5
*
TOTAL 460 100.0 100.0
MISSING CASES 264
-QF TUB OLE AM I N«~"' '
DCl ATTWCT 7n ilfeTCTi
ABSOLUTE FREQ FREQ
CODE FREQ (PCT) (PCT)
A 62 13.5 14.0
R ?"3P e^J 7 c;-^ £
C 133 28.9 30.0
0 11 2.4 2.5
' * ^ ^
TOTAL 460 100.0 500.0
MISSING CASES 16
FREQ
(PCT)
76.0
99.5
100.0
i U • -.
FREQ
(PCT)
14.0
A7 ft
9.7.5
100.0
i 0 f > n
<
254
-------
: (53/21/78
FILE -•INK
- CREATED 03/21/78
1 . .
CATEGORY LABEL :
ALL OF THE TIME
MOST OF THE TIME
OCCASSIONALLY
NEVER :
it
VALID CASES 297
V Q5.9 ..: REUSE SPEMT-
f
CATEGORY LABEL
ALL OF THE TIME
MOST' OF THF TTMF;
OCCASSIONALLY
NEVER
i VALID CASES , 296 "
V. Q60 SPILL CLEAN
CATEGORY LABEL •
1
1 YES
j NO , •.. .,..'
L
:
CODE
A ,
R
C
0
TOTAL
ABSOLUTE
FREQ
12
14
34
237
163
460
RELATIVE ADJUSTED
FREQ FREQ
(PCT) (PCT)
2.6
7.4
51.5
• •
100.0
4.0
4.7
11.4
79.8
—MISSING-
ioo.o
CUM
FREQ
(PCT)
4.0
fl.fl
20.2
100.0
100,0
MISSING CASES 163
RINSE. WATER As WACH WATER
ad ATTl/IT
CODE
A
R '
C
o ;
TOTAL
MISSING
UP BY DRY
COOE
A
B •
TOTAL
ABSOLUTE
FREQ
46
40
172
460
CASES 164
METHODS
ABSOLUTE
FREQ
363
27
460
-1
FREQ
(PCT)
10.0
a, 3
8.7
37.4-
•^c; 7
100.6
RELATIVE
FREQ
(PCT)
78.9
1S.2_
5.9
106.0 -
ADJUSTED
FREQ
(PCT)
15.5
13.5
58.1
M I 3 3j Wj
100.0
... ADJUSTED
FREQ
(PCT)
83.8
16.2
MISSING.
100.0
/*» IM
FREQ
(PCT)
15.5
41.9
100.0
i n A rt
.— ... .CUM : ..
FREQ
' (PCT)
83.8
i rtn n
100.0
i
i - VALID CASES
433
MISSING CASES
255
-------
03/21/78
FILE - INK
- CREATED 03/21/78
s 0^1 FI nno ni?ATMC ' Tn ^TODU CFUFD •
i
CATEGORY LABEL
YES
wn
VALID CASES
> 062 FLOOR
CATEGORY LABEL
-""YES""'
rn
y
VALID CASES
1
v 053 UATED
CATEGORY LABEL
0 TO 5
f, Trv \n
11 TO 50
' YA LID- .CASES
DFLATTVF
ABSOLUTE FREQ
CODE FREQ (PCT)
A 61 13.3
R- TA7 70. B
"32 7,0
TOTAL 460 100.0
428 MISSING CASES 32
DRAINS CONNECTED TO SANITARY SEWER -
"FLATIVF
ABSOLUTE FREQ
CODE FREO (PCT)
A 170 37.6
27 ' 5.9
TOTAL 4bO 100.0
433 MISSING CASES 27
I i^FD Tn UJRCU i TO in CAI TI ics
-AOJUSIEO
FREQ
(PCT)
14.3
RE;, 7
MISSING
1.00.0
ADJUSTED
FREQ
(PCT),
39.3
MISSING
100.0
("I !M
FREQ
(PCT)
14.3
1 0 n . 0
100.0
(^11M ' '
FREQ
(PCT) j
39.3
1
1000 ;
ioo.o •
DC! ATT\/C" An MfCTtm ^»«iui
ABSOLUTE FREQ FREQ
CODE FREQ (PCT) (PCT)
A 162 35.2
R J £t. 3 i 0
C 4 0.9
280 60.9
T^TAL ^^n inn o
isn MTc^TKir ra^P9 *
90.0
7 a
2.2
MISSING
inn n
FRFQ
(PCT)
90.0
100.0
100.0
256
-------
03/21/78
FILE - INK
- CREATED 03/21/78
s~
CATEGORY LABEL
0 TO 5
6 TO 10
11 TO 50
51 TO 100
QVFR ino
VALID CASES 226
ABSOLUTE
CODE FREQ
A 168
B 40
c is
0 2
234
TOTAL 460
MISSING CASES 234
RELATIVE-..
FREQ
(PCT)
36.5
3.3
0.4
0.2
50,9
100.0
ADJUSTED
FREQ
(PCT)
74.3
17.7
6.6
0.9
0.4
MISSING
100.0
CUM
FREQ
(PCT)
74.3
98.7
99.6
100.0
V
-
r
i
Q65 U"\TEO USE™ Tn
CATEGORY LABEL
0 TO 5
ft j<"> \n
11 TO 50
51 TO 100
\
—OVER- 100
\
VALID CASES 204
fJACUA C 1 TH Irtrt rtAI
ABSOLUTE
CODE FREQ
A 128
g ^T
C 28
D ; "3
E ' 2
256
TOTAL *60
MISSING CASES 256
T'JR
DILATIVE
FREQ
(PCT)
27.8
o 3
6.1
0.7
0 4
55.7
ioo.o
ADJUSTED
FREQ
(PCT)
62.7 .
21.1
13.7
1.5
1 0
MISSING
100.0
CUM
FREQ
(PCT)
62.7
97.5
99.0
100.0
257
-------
L
03/21/78 FILE - INK - CREATED 03/21/78
._Q66.
1
CATEGORY LABEL
0 TO 5
6 TO in
11 TO 50
51 TO i6o
nvFR Tnn
VALID CASES 155
> 0^7 W*TED ' '5ED
\
CATEGORY LABEL
0 TO 5
U TO 50
51 TO 100
n\/£p - 1 o 0
VALID CASES 105
CODE
A
s
c
D
r
TOTAL
MISSING
TO WASH *\ ^5
CODE
A
R
C
D
£
TOTAL
MISSIWG
ABSOLUTE
FREQ
87
37
5
I
305
460
CASES 305
1 Tn 500 GA
ABSOLUTE
FREQ
70
If,
• 13
4.
2
. 355
460
l_ 1 UO
RELATIVE
FREQ
(PCT)
18.9
8.0
i.i
66.3
100.0
L TUB
RELATIVE
FREQ
(PCT)
15.2
2.8
• 0.9
77.2
100.0
An »i<;TFn rt IM
FREQ FREQ
(PCT) (PCT)
56.1
1 ft . 1
23.9
3.2
MISSING
100.0
FREQ
(PCT)
66.7
12.4
3.8
MISSING
ioo.o
56.1
96.1
99.4
1
100,0
-J
FRE'Q
(PCT)
66.7
94.3
98.1
100^0
100.0
CASES 355
a
258
-------
1
03/21/7ft
FILE - INK
- CREATED 03/21X78
>..Q6a-._ WATER USED TO WASH A 501 TO 1000 GAL TU
•
- . - ABSOLUTE
CATEGORY LABEL CODE FREQ
.. 0 TO 5 . : A 56
6 J0...1.0 . .. . q •*
11 TO 50 i C 3
1 51 TO 100 D 5
<»s
TOTAL 460
VALID CASES 69 MISSING CASES 391
^ — QA-*3 VATF." "^F_n TO WASH A 1000 GAL nP M
ABSOLUTE
CATEGORY LABEL CODE 'FREQ
0 TO 5 A : 46
6_T_0_. 10: 91
11 TO 50 C 2
51 TO 100 D 1
QVFR inn E j
-*«.
TOTAL 460
VALID CASES 52 MISSING CASES 408
Dpi ATTUP
FREQ
(PCT)
12.2
n.7
0.7
i»i
0.4
.85.0
10 0.0
nop- -rii
RELATIVE
FREQ ""
(PCT)
10.0
0.2
0.4
.0.2
88.7
100.0
A n II tcTtrn
FREQ
(PCT)
\
81.2
4.3
4.3
7.2
MISSING
100.0
API iiiQTPri
FREQ
(PCT)
88.5
i Q
3.8
1.9
MISSING
100,0
- CUM
FREQ
(PCT)
81.2
89.9
97.1
inn n
100.0
Pi 'M
FREQ
(PCT)
88.5
QQ &
94.2
96.2
i nh n
100.0
•
......
259
-------
03/21/78
FILE - INK
- CREATED 03/21/78
"ELATTVP
ABSOLUTE FREQ
j CATEGORY LABEL CODE FREQ (PCT)
| YES A 38 8.3
-NO R 311 A7.A
1.11 24.1
! TOTAL 460 100.0
t
VALID CASES 349 MISSING CASES 111
V OT1 TC CDI V/FMT DPnTCTTI I crn OMCTTC
ABSOLUTE FREQ
CATEGORY LABEL CODE FREQ (PCT)
YES A 2 0.4-
MO R 7AA. yq . 1
94 20.4
TOT4L 460 100.0
VALID CASES 366 MISSING CASES 94
V 07? ,, IS STtAM INJECTION! DISTILLATION USED
, , "RELATIVE
ABSOLUTE FREQ
CATEGORY LABEL CODE FREQ (PCT)
NO 8 55 12.0
1 *
TOTAL 460 100.0
f
, VALID CASES 55 MISSING CASES 405
i
1
v^
. ADJUSTED -
FREQ
(PCT)
10.9
MISSING
100.0
FREQ
(PCT)
0,5
MISSING
100.0
ADJUSTED
FREQ
(PCT)
100.0
MISSING
100.0
CUM
FRFQ
(PCT)
10.9
inri.n
100.0
(PCT)
0.5
1 n n , n
100.0
n IM
FREQ
(PCT)
100.0
1 nn . n
260
-------
03/21/78
FILE - INK
.- CREATED 03/21/78
i
CATEGORY LABEL
VAI in rA
-------
03/21/78
> QZ6 _. STEAM
CATEGORY LABEL
YES
VALID CASES
> H77 STEftW
CATEGORY LABEL
YES
VALID CASES
FILE - INK f CREATED 03/21/78
CONDENSATE MIXED WITH PROCESS WAST
... _.. RELATIVE
ABSOLUTE FREQ
CODE FREQ (PCT)
D 1 0.2
4=?Q tJQ.^fl
TOTAL 460
1 MISSING CASES 459
COMDEMSATE DISPOSED OF OTHER
1
ABSOLUTE
CODE FREO
E 3
TOTAL 460
3 MISSING CASES 457
ioo.6
METHO
3EL-AT-I-V-E—
FREQ
(PCT)
0.7
' QQ , 3
100. 0
ADJUSTED-
FREQ
(PCT)
— ;
. , CUM
FREQ
(F'CT)
100.0 100.0
..MISSING IOfl.0 ,!.,,
100. 0
,-AOJUSXEO-
FREQ
(PCT)
100.0
MISSING
100.0
CUM-..,- , ,
FREQ
(PCT)
100.0
100^0
'.
1 •
L rV7fl SPFNT
1
CATEGORY LABEL
YES
Kin
™u .
i VALID CASES
CAUSTIC TO SANITARY SEWER
ABSOLUTE
CODE FREQ
A 43
8 . lag...
22B
TOTAL 460
RELATIVE
FREQ
(PCT)
9.3
.41.1- -
49.6
ioo.6r
ADJUSTED CUM
FREQ FRFQ
(PCT) (PCT)
18.5
81.5
MISSING
100.0
18.5
100.0
100.0
232 MISSING CASES 228
262
-------
03/21/78 FILE - INK , .; - CREATED 03/21/78
- Oza SPENT SCM^gM"^ TO e;A\iYYApY SEWFO
; — ^ . . DPI ATTWIT
• ABSOLUTE FRFQ
CATEGORY LABEL CODE FREQ (PCT)
YES A 26 5.7
.60 13.6
TOTAL 460 100.0
VALID CASES 400 MISSING CASES 60
}».. 080 .WET SCRUBBERS USED FOR AIR POLL
:
_ , . . - ABSOLUTE FREQ ^
CATEGORY .LABEL CODE FREQ (PCT)
y£S A 10 2.2
NO - • B 4?T 9\ 1
« 29 6.3
TOTAL 460 100.0
VALID CASES 431 MISSING CASES 29
1 .. ._^ , .. . . ' ...;.. . _
CATEGORY LABEL COOE ^FREO^ "c?>
l~Yes - . •: « i — —^r~
— — ^57 9O.T
TOTAL 460 100.0
— AO-JU5TED-
FREQ
(PCT)
, 6.5,
MISSING
100.0
ADJUSTED—
FREQ
(PCT)
2.3
97.7
MISSING
100.0
-ADUU-SZEO—
FREQ
(PCT)
ioo.o
M T CC T Mi"
100.0
CUM — ,
FREQ
(PCT)
6.5
1 ft ft ft
100.0
,
FREQ
(PCT)
2.3
100 n
100.0
CUM-
FRFQ
(PCT)
100.0
_1 n n . n
— — : . , .
VALID CASES
r
MISSIMG CASES 457
263
-------
03/21/78
FILE - INK
CREATED 03/21/78
S Q82-
..USE OF ELECTROSTATIC PRECIPITATORS
RELATIVE...
ABSOLUTE FREQ
CATEGORY LABEL CODE FREQ (PCT)
YES B 2 0.4
— - - • • • • • • •
TOTAL 460 100.0
VALID CASES 2 MISSING CASES 458
"ELATIVE
ABSOLUTE FREQ
CATEGORY LABEL CODE FREQ (PCT)
YES C 99 21.5
TAI 70.=;
TOTAL, 460 100.6
VALID CASES 99 MISSING CASES 361
OftA HCF OF CYCLQNFS - ... - -
.ADJUSTED CUM.
FREQ FREQ
(PCT) (PCT)
ioo.o ' ioo.o
..MISSING 100.0
.
100.0
ADJUSTED rUM
FREQ FREQ
(PCT). (PCT)
ioo.o iooao
100.0
CATEGORY LABEL
"YES
RELATIVE -ADJUSTED CUM.
ABSOLUTE FREQ FREQ FREQ
CODE FREQ (PCT) (PCT) (PCT)
TOTAL
7 1.5
_4S3 98.5.
460 100.0
100.0 100.0
MISSING —.100..0—
100.0
VALID CASES
MISSING CASES 453
264
-------
;> OSS
03/21/78 FILE - INK - CREATED 03/21/78
"SF OF FTLTFTPS Fnn_ATP Pni t rnMTonL
CATEGORY LABEL
CODE
-BELAT-IYE—ADJUST
FREQ FREQ
(PCT) (PCT)
21.1 ,100.0 100, n
-Z8*S MISSIHG 1-0-Q-»Q_
TOTAL
460
100.0
100.0
VALID CASES
97
MISSING CASES 363
QQT
CATEGORY LABEL
ABSOLUTE
CODE FREQ
JLJtT-J-WE—AOJJJSXEO CUM-
FREQ FREQ FREQ
(PCT) (PCT) (PCT)
YES
TOTAL
5 1.1 100.0 100.0
—ASS—'. ...98.9—. —-MISSJJSIG 1_Q..Q...^O_
460 100.0 100.0
VALID CASES
MISSING CASES 455
—_Q88 —
--BOILER SLOWDOWN COMBINED
CATEGORY LABEL
YES
..—.-.: __-_.-:• RELATIVE ADJUSTED-... .CUM
ABSOLUTE FREQ FREQ FRfQ
CODE FREQ (PCT) (PCT)
B
TOTAL
460
7 1.5 100.0 100.0
__98.5..._ MISSING 100.0..
100.0 100.0
VALID CASES
7
MISSING CASES 453
265
-------
03/21/78
f
\
CATEGORY LABEL
YES
VALID CASES
^ Q90 NON CO
CATEGORY -LABEL
VALID CASES
V. AO1 CAMTT/i
CATEGORY LABEL
YES
VALID CASES
FILE - INK - CREATED 03/21/78
CLEAMTMG VM5TE COM°lMEr*
ABSOLUTE FPEQ FREQ
CODE FREQ (PCT) (PCT)
C 4 0.9 100.0
456 QQ . T Mi«s^f-N<7
TOTAL 460 ioO.O 100.0
4 MISSING CASES , 456
N. nf+f f*nni*T"Mft UATPR rTlMRTKlFH , ...
RFI.ATJVF ADJUSTEE
ABSOLUTE FREQ ' FREQ
CODE FREQ (PCT) (PCT)
0 46 10.0 100.0
414 90^0 MISSING
TOTAL 460 100.0 lOO.O
46 MISSING CASES 414
pv WAST^rf/TE0 '"CM0 1 MED
PEL*TT-yp" — tTLJli^TPJ
ABSOLUTE FREQ FREQ
CODE FREQ (PCT) (PCT)
E , 41 8.9 100.0
TOT4L 460 100.0 100.0
41 MISSING CASES 419
1
I
CUM
FREQ
(PCT),
100.0
i no . £i
-
1 OJM
FREQ
(PCT)
100.0
lon.n
^
FRPQ
(PCT)
100.0
100.0
i
266
-------
03/21/78
FILE - INK
- CREATED 03/21/78
..LABORATORY WASTEWATER COMBINED
CATEGORY LABEL
YES
VALID CASES 21
^ CL9-T ^TEAM CWf
s CATEGORY LABEL
VALID CASES 5
^ ooe; wni YlMP nc
CATEGORY LABEL
0
1 TD inn fipn
101 TO 250
251 TO 500
751 TO 1000
OVER 1000
'
CODE
F
i
TOTaL
MISSING
CODE
•G ;
TOTAL
MISSING
TMK ppnpjree;1 I
CODE
A
R
c
D ,
F ;
G
TOTAL
\
ABSOLUTE
FREQ
21
460
CASES 439
ABSOLUTE
FREQ
5
460
CASES 455
ABSOLUTE
FREQ
171
171
33 •
12
5
12
50
46"0
RELATIVE
FREQ
(PCT)
4.6
ioo.o
RELATIVE
FREQ
(PCT)
1.1
QQ m O
100.0
T^D GP
PELATI VE
FREQ
(PCT)
37.2
"*7 • 2
7.2
2.6
1.3
v.i"
, 2.6
i n .0
100.0
ADJUSTED
FREQ
(PCT)
100.0 ,
MISSING
100.0
An II icTrn
FREQ
(PCT)
100.0
3
ioo.o
ADJUSTED
FREQ
(PCT)
41.7
M.7
8.0
2.9
1 *5
1.2
2.9
MISSING
100.0
1
FREQ
(PCT)
ioo.o
100.0
CUM
FREQ
(PCT)
ioo.o
inn n
CUM
FREQ
(PCT)
41.7
9i.5
94.4
QC; o
97.1
100.0
1 nn n
.,
267
-------
03/21/78
FILE - INK
- CREATED 03/21/78
y...Q96 . . PEAK VOLUM
CATEGORY LABEL
0
1 TO TOO
-------
03/21/78
-09.9..
FILE - INK
- CREATED 03/21/78
U)flc;TFWATP-0
REUSED
CATEGORY LABEL
REL A-T-I-VE ADJUSTED CUM—
ABSOLUTE FPEQ- FREQ FREQ
CODE F.REQ (PCT) {PCT) (PCT)
YE?
45
415
9.8 100.0 100.0
Q.g MIS?INQ 100.0
TOTaL
460
100.0
100.0
VALID CASES
45
MISSING CASES 415
- Q1QO.-
-WASTEWATER DISCHARGED
•TO CITY SEWE
CATEGORY LABEL
"YES ~
.. . ; . , .._. - . .. RELATIVE __ ADJUSTED
ABSOLUTE FREQ FREQ
CODE FREQ (PCT)
FRFQ
(PCT)
138
_322_
TOTAL
460
30.0 100.0
-,_7..0,«J1 MISSING-
100,0 100.0
100.0
Tnn.o
VALID CASES
138
MISSING CASES 322
CATEGORY- LABEL
YES
i
ABSOLUTE
CODE . FREQ
E 13
447
TOTAL 460
RFLATIVE
FREQ
(PCT)
2.8
Q7.2
100.0
— AOJUSI£D-
FREQ
(PCT)
100.0
MISSING
100.0
ryM
FRFQ
(PCT)
100.0
i nn n
VALID CASES 13 MISSING CASES'' 447
269
-------
03/31/78
FILE - INK
- CREATED 03/21/78
-WASTEWATER DISCHARGED TO RECEIVING WATER
CATEGORY LABEL
YES
RELATIVE.
ABSOLUTE FREQ
CODE FREQ (PCT)
F 4 6.9
CUM._
FREQ FREQ
(PCT) (PCT)
TOTAL
460
100. 0
1.00.0 1QQ..O
SS.ING -.LOJU-Q-
ioo.o
VALID CASES
MISSING CASES 456
Q103
CATEGORY LABEL
CODE
BELAJ3-UE AOJUSXEO——CUM_
ABSOLUTE FREQ FREQ. FREQ
FREQ
;(PCT)
(PCT)
(PCT)
YES
3.0
100.0
100.0
-1.0.(U-0-
TOTAL
460
100.0
100.0
VALID CASES
14
MISSING CASES 446
I
CM-Q4-
-WASThWATER INCINERATED
CATEGORY LABEL
"YES"'""
VALID CASES
. RELATIVE.... ADJUSTS!
ABSOLUTE FREQ FREQ
CODE FREO (PCT) (PCT)
H
0.4
TOTAL 460 100.-0
MISSING CASES , 458
100.0
.-MISSING.
100.0
_.._CUM_
FRFQ
(PCT)
f.pci.o
_1.0\0 . 0^_
270
-------
03/21/78 i FILE
^ m n=; WACTFWATFO m
CATEGORY LABEL
YES
VALID CASES 2
y, — QID.O WASltWAItK LI
CATEGORY LABEL
YES
VALID CASES 123
L qin7 UACTFUATFD 1
CATEGORY LABEL :
YES ;
- INK - CREATED 03/21/78
RELATIVE ADJUSTED CUM
ABSOLUTE FREQ FREQ FREQ
CODE FREQ (PCT) (PCT) (PCT)
I 2 0.4 100.0 100.0
... ...
TOTaL 460 100.0 100.0
MISSING CASES 458
^MTO A f*T LI A 1 It m — .
RELATIVE.'- ADJUSTED- -CUM
ABSOLUTE FREQ ' FREQ FREQ
COf)E FREQ (PCT)
-------
03/21/78
FILE - INK
- CREATED 03/21/78
1
V— oinft WftST^WATE0 TO DEEP WFLL DISPOSAL
'
RFLATT VF
ABSOLUTE FREQ
CATEGORY LABEL CODE FREQ (PCT)
YES L 1 0.2
TOTAL 460 100.0
VALID CASES 1 MISSING CASES 459
V nifiQ- AycofiRP \/o[_i IMC TMi'' PR^^E^S W^^TE DISCH^P
"tl_ATT^E
ABSOLUTE FREQ
CATEGORY LABEL CODE FREQ (PCT)
0 A .237 51.5
1 yn ]hn GPD n si 1^,3
101 TO 250 C 32 7.6
251 TO 500 D 10 2.2
=;oi -f " 7^1 E * 1*1
751 TO 1000 F 5 1.1
OVER 1000 G 11 2.4
7* 1*.5
TOTAL 460 100.0
VALID CASES 384- MISSING CASES 76
ADJUSTFD
FREQ
(PCT)
100. 0
-MISSING
100.0
AOJ"STED
FREQ
(PCT)
61.7
8.3
2.6
1.3
1.3
2.9
-M.ISSI-NG -
100.0
PI IM '
FREQ
(PCT)
100.0
100 ft
(PCT)
61.7
AT .A
91.9
t
94.5
97.1
100.0
loii.o
\
272
-------
03/21/78
FILE - INK
- CREATED 03/21/73
i.
CATEGORY LABEL
0
1 TO 1 0..0 .GI2D _
101 TO 250
251 TO 500
f?m Tn 7SO
751 TO 1000
OVER 1000
VALID CASES
; - RELATIVE -
ABSOLUTE FREQ
CODE FREQ (PCT)
A 209 45.4
- .. B i 7j 15,4-
C 26 5.7
D 18 3.9
F A pta
F 3 0.7
\ ' G 12 2.6
117 25.4-
TOTAL 460 100.0
343 MISSING CASES 117
ADJUSTED--.
FREQ
(PCT)
60.9
7.6
5.2
1.2
0.9
3,5
100..0
FREQ
(PCT)
60.9 '
89.2
94.5
96.5
100.0
1 00 ft
i : .
.... ..
QI i 1 nnc-c
f "J-J-i u^i_J
"CATEGORY LABEL
YES
NO
VALID CASES
PLANT HAVE MPPFS PERMIT
RELATIVE
ABSOLUTE FREQ
CODE FREQ (PCT)
A 10 2.2
> 359 78.0
TOTAL 460 100.0
. ,101 MISSING CASES 359
-ADJUST-ED—
FREQ
(PCT)
9.9
e>n , i
MISSING
100.0
riiM
FPEQ
(PCT)
9.9
100.0
100.0
-
I . '
' ' " -
273
-------
03/21/78
O}
FILE - INK
- CREATED 03/21/78
ABSOLUTE
CATEGORY LABEL CODE FREQ
YES 'A 8
NO R ?|A
236
TOTAL 460
RELATIVE
FREQ
(PCT)
1.7
51..3
100.0
ADJUSTED—
FREQ
(PCT)
3.6
96,4
MISSING
100.0
—. '
FREQ
(PCT)
3.6
i n n , o
100.0
VALID CASES 224 MISSING CASES 236
> llf"^ nnfTQ PLANT H*VE'DFPMTT FOP.,COOLiKIG
ABSOLUTE
CATEGORY LABEL C05E FREQ
YES A ig
NCI R 91 R
223
TOTAL 460
WATE°
PELATIVE *n.iiicTPn
FREQ
(PCT)
4,1
47, i.
43.5
100.0
FREQ
(PCT)
a.o
O9, 0
MISSING
100.0
: run
FREQ
(PCT)
8.0
100,0
ioo.o
VALID CASES 237 MISSING CASES 223
V Q_1_1_q UtlMTr-[0*]_TTy ncpc; WA^T^ nopi
_ , ABSOLUTE
CATEGORY LABEL CODE FREQ
YES A 84
-
TOTAL 460
NAMTE
DPI ATTUF
FREQ
(PCT)
18.3
*
100.0
— ivOJUSIEO —
FREQ
(PCT)
100.0
ioo.o
f*l IM
FRFQ
(PCT)
100.0
i n o o
VALID CASES 84 MISSING CASES " 376
274
-------
j 03/21/73 FILE - INK - CREATED 03/21/78
y.-.QU.6— _ MUNICIPALITY IMPOSES SEWER USE CHARGES
CATEGORY LABEL
, ~YES "~~ 7 ".
-....., , __.-— , RELATIV£-_. AD JUSTED CUM_
ABSOLUTE FREQ FREQ FREQ
CODE FREQ (PCT) (PCT) —Q-ua—: MUNICIPALITY
ISSUES SEWER PERMITS
CATEGORY LABEL
YES •
s. .___—_._._; ....RELATIVE- ADJUSTED CUM_
ABSOLUTE FREQ FREQ FREQ
CODE FREQ (PCT) ' (PCT) (PCT)
39
8.5
100.0
100.0
-,_9..1..5 MISSING LQ.O..Q
TOTAL
460
100.0
100.0
VALID CASES
39
MISSING CASES 421
275
-------
03/21/78
FILE - INK
- CREATED 03/21/78
MIJMICIoaLTTv "EO'-'IPEg PLAMT TO A.MALYZE! ''/
CATEGORY LABEL
RELATJl-y£-
ABSOLUTE FPEQ
CODE FREQ (PCT)
FREQ
(PCT)
F=cFQ
(PCT)
YES
30
6.5
100.0
100.0
TOTAL
4-60
100. 0
100.0
VALID CASES
30
MISSING CASES 4^u
O1 7>Q
..PLANT WASTEWATER IS TREATED BEFORE DISPO
CATEGORY LABEL
VALID CASES
.231
1 RELATIVE—ADJUSTED CUM_
ABSOLUTE FREQ FREQ FREQ
CODE FREQ (PCT) (PCT) „ (PCT)
A
_ B __.
TOTAL
30
?01
. 22?
460
6.5
43.7
49.8
100.0
13.0
aytn
MISSING
100.0
13.0
100,0
MISSING CASES 229
276
-------
03/21/78
FILE - INK
- CREATED 03/21/78
:__i: PFf ATTVF AR PM^TPn
. -'- ABSOLUTE FRFQ FREQ
CATEGORY LABEL CODE FREQ (PCT) (PCT)
0 A 78 17.0 78.0
1 TO ?n R 7 i i*- 7 n
.21 T0 4« C 3 0.7 3.0
41 TO 6Q 0 1 , 6.2 1.0
- «-f- T.n CJQ '"~ F ; ? ^ 4 p 0
100 G 9 2.0 9.0
360 78,3 MISSING
TOTflL ^6" inf 0 inn n
tfAMD CASFS 100 _MlAsiwa CA?;Ft; 7Arj
)
\
'
P1 (M
FREQ
(PCT)
78 ..0
88.0
89.0
Q| f)
100.0
100.0
-
I
^—CLL22 : RESIN WASTE AS PERCENT OF TOTAL
. -- •
CATEGORY LABEL
°
.LJT0...20 '• ...
— - - ——^—>- --•- RELATIVE— ADJUSTED CUM_
ABSOLUTE FREQ FREQ FREQ
CODE FREQ (PCT) (PCT) (PCT)
70
15.2
TOTiL
388
460
84.3
100.0
97.2 97.2
2.8 LOO.O..
MISSING -10-0.0
100,0 ~~ ~~"
VALID CASES
72
MISSING CASES 398
277
-------
03/21/78
FILE - INK
- CREATED 03/21/78
"
ABSOLUTE
CATEGORY LABEL CODE FREQ
0 A 95
ion ft i
TOTAL 460
VALID CASES 96 MISSING CASES 364
_
01 ?4 ATP PfH | WA^TF AS PFprFNT OF TOTAf
i
1
i
! ABSOLUTE
CATEGORY LABEL CODE FREQ
0 A« 73
! 1 TO ?0 8 f
386
JU
'ELATIVE
FREQ
(PCT)
20.7
n,?
7Q.T
100.0
BELATXVE-
FREQ
(PCT)
15.9
83.9
AOJH5TPD
FREQ %
(PCT)
99.0
MISSING
100.0
AO-JU«;TFn
FREQ
(PCT)
98.6
1.4
MISSING
/ ;
FREQ
(PCT)
99.0
loo. n
100.0
i
'
FREQ
(PCT)
98.6
i o n „ n
100.0
TOTAL
460
100.0
100.0
VALID CASES
74
MISSING CASES 386
278
-------
03/21/78 FILE -
> — 04-25 gA"TTAPY- WASTE.
CATEGORY LABEL
o
i rn po
21 TO 40
100
VALID CASES 129
INK - CREATED 03/21/78
_a.9 pro'^frivif AF TOT/iL
OPM ATTW1T
ABSOLUTE FREQ
CODE FREQ (PCT)
A 1.17 ,25.4
.. . B : L. no
C 4 0.9
G . t. 4 ••- 0.9
TOTAL 460 100. 0
MISSING CASES 331
— AOJUS-TED-
FREQ
-(PCT)
90.7
*3 1
i » 1
3.1
3.1
— M-I55IN6 — _
100.0
-.
CUM
FRFQ
(PCT)
90.7
96.9
100.0
— U)0 , 0 ;
• ' .
• i •-''..
^ — QI2.6 — -- -. COOLING WATER, A
CATEGORY LABEL
_ ________
1 TO ?Q
21 TO 40 .
41 TO 60
• 6.1 T0_ 80
81 TO 99
100 i
S PERCENT. OF TOTAL
DC*I ATTl/C*
ABSOLUTE FREQ
CODE FREQ (PCT)
A 122 26. S
8 P n j
C 1 0.2
D , 2 0.4
F ; >, 0.9 '
•• « ,5 1.1
..oS^-H.
TOTAL 460 100.0
-ADJUSTED—
FREQ
(PCT)
87.8
1 -4
0.7
1.4
2.9
3.6
100.0
FREQ
(PCT)
87.8
flQ 5
89.9
91.4
Q-3 C
96.4
100.0
IQO^Q
VALID CASES
139
MISSING CASES 321
279
-------
03/21/73
FILE - INK
- CREATED 03/21/78
y Ql?7 njM^M wnv | fc n^ — tdfaWUf-f^-J — •*-«= ULM-O-U
i
ABSOLUTE
CATEGORY LABEL CODE FREQ
0 A 39
1 TO ?0 R 1
81 TO 99 F 1
. *.l?
TOTAl A Art
Mt-aiiBJ*™-' ii
nioft TPFATMFMT RY WFHTPAI T7ATTOM
ABSOLUTE
CATEGORY LABEL CODE ' FREQ
,' YES A 9 '
45 V
TOTAL 460
| VALID CASES 9 MISSING CASES 45
.
,_-,.
ABSOLUTE
CATEGORY LABEL " CODE FREQ
YES 8 36
4?4
TOTAL 460
"""-•- • — "
-BELAXIVE AOJUSXED—
FREQ FREQ.
(PCT) (PCT)
8.5 95.1
0.2 2.4
.91.1. MISSING
inn.o ion, n
Q
RE'LAT IV.E AD JUS3^D_
FREQ FREQ ,
(PCT)
-------
Q3/21/7B
FILE - INK
- CREATED 03/21/78
-Q130 TREATMENT BY FLOTATION
CATEGORY LABEL
• RELATIVE ADJUSTED
ABSOLUTE FREQ FRFQ
CODE FREO (PCT) (PCT)
CUM._
FREQ
(PCT)
1 460 loo.o MISSING 100.0
— : -;-'- ..—TOTAL 46<3 iO.O*jQ_. 100.0
— .VAL1D_CASES.._. ..0 MISSING CASES.. . 460 "_
J • • - . — - . • ;
•f Q13] TOFflTMFMT HV pr)LYMER_
- - - I •
~ : — — : BELATIME An.iilgTFn ryM
PATFrnov , -Xan ' , . _' ABSOLUTE FREQ FREQ FREQ
CATEGORY LABEL CODE FREQ1 (PCT) (PCT) (PCT)
• •"• v : • ^66 foo.p MISSING 100.0
— TOTAL 4^Jl______LaQ^JL 1-0 OyQ. '
—VAI TD CASE.S : _Q MT^-.Mn TA<;F<; ^.An "'
^ Q132— LAGOON TREATMENT " ^ .
.._._. ..... ' ,.. ... .. .. . .,...,_,. RELATIVE ADJUSTED CUM._.
• . _'. ABSOLUTE FREQ FREQ FREQ
CATEGORY LABEL CODE ; FREQ (PCT) (PCT) ' (PCT)
E 3 0.7 .100.0 100.0
— , „-_,.; ,.'. 457. .99.3 _'. MISSING- -_1.00..0_.,
TOTAL 460 ~100.0 100.0
VALID CASES
MISSING CASES 457
281
-------
03/21/78 rILE - INK - CKtATtU OJ/dl/ra
V Ql 3^ CADPO^I Ap^npoy^nM TD^^TMFMT
c
RH.&TTVF AQJUSTF_D_
ABSOLUTE FREQ FREQ
CATEGORY LABEL CODE FREQ (PCT) (PCT)
460 100,0 MISSING
TOTAL 4fin inn,n inn, ft
O1**4 TREATMENT BY FQUAl'lZATION • • ......... ..
RELATIVE ADJUSTED ..
ABSOLUTE FREQ FREQ.
CATEGORY LABEL CODE FREQ (PCT) (PCT)
YES G 3 0.7 * .100.0
4^7 " 99.J3 MISSING—
TOTAL 460 iOQ.O 100.0
VALI.D CASES 3 MISSING CASES 457
FREQ
(PCT)
lOOoO
CUM
FREQ
(PCT)
100.0
_LCLQLJ5 :
CATEGORY LABEL
YES
VALID CASES 11
ABSC
CODE FF
H
t
TOTAL l
MISSING CASE
RELA-T-I.VE ADJUSTED CUM_
ABSOLUTE FREQ FREQ . FREQ
(PCT) (PCT) (PCT)
46.0
100.0 10000
x MISSING 1.00 ,.0-
100.0 100.0
r
282
-------
L
r
.
1
1
r
r~
\
03/21/79 ' . FILE - INK - CREATED
Q13o TWt.AfMc.NI H Y LI"t, AUD I i iUN
ABSOLUTE
CATEGORY LABEL > COnE FREQ
460
TOTil 460
': ' •' :
. .. ...
ABSOLUTE
CATEGORY LABEL CODE FREQ
YES .- J 1
.
, TOTAL 460
VALID CASES 1 MISSING CASES 45
QU38 TREATMNT BY GRAVITY SEPARATION
: , - . ABSOLUTE
CATEGORY LABEL CODE FREQ
YES ; K '• 19
_. ._.„.., . ; . ' ' ... _... '. .._ ..441
TOTAL 460
03/21/78
RELATIVE
FREQ
(PCT)
100.0
ioo.o
D
RELATIVE
FREQ
,(PCT)
0.2
QQ.fl
100.0
9
RELATIVE
FREQ
(PCT)
4.1
95.9
100.0
1
ADJUSTED
FREQ
(PCT)
MISSING
100,0
i
-ADJUSTED
FREQ '
(PCT)
100.0
RISSiNG.
100.0 '
-
ADJUSTED
FREQ
(PCT)
100.0
MISSING
100.0
CUM
FREQ
(PCT)
100.0
-
CUM
FREQ
(PCT)
100.0
100.0
•• "
CUM
FRFQ
(PCT)
100.0
100.0
i
'VALID CASES
19
MISSING CASES 441
283
-------
] 03/21/78
FILE - INK
-IB£AJMFNT RY FILTPAJJpJM-
- CREATED 03/21/78
CATEGORY LABEL
RELATIVE-—ADJUSTED CUM_...
ABSOLUTE FRF.Q FREQ FREQ
CODE FREQ (PCT) (PCT) (PCT)
f YES
0.9 100.0 100.0
JG LQ.OL»G-
TOTaL
460
100.0
100.0
VALID CASES
MISSING CASES 456
i
>-._ai.40 .... _.. TREATMENT BY ALUM ADDITION
CATEGORY LABEL
YES
ABSOLUTE
CODE FREQ
RELATIVE ADJUSTED CUM...
FREQ
((PCT)
FREQ
(PCT)
FRF.Q
(PCT)
M
TOTAL
Z
460
0.4 100.0
^-99.6. -...MISSING.
100.0 100.0
100.0
-1Q.O..O_
VALID CASES
MISSING CASES 458
> CO.4J.
apTTVATPn g|"P?F TPFXTMFMT,
CATEGORY LABEL
"YES
; , RELATIVE—ADJUSTED C
ABSOLUTE FREQ FREQ FRFQ
CODE FREO (PCT) (PCT) (PCT)
TOTAL
460
1.5 100.0 100.0
—98 ..5 MISS ING 10 0 ..0
100,0 100.0
VALID CASES
MISSING CASES 453
-------
03/21/73
FILE -
- CREATED 03/21/78
Q142
BATCH OR CONTINUOUS TREATMENT SYSTEM
CATEGORY LABEL
BATCH
CONTINUOUS _..
1 '
CODE
A S
B
0 i
•OTAL
. ABSOLUTE
FREQ'
34
27
399
460
RELATIVE
FREQ
(PCT)
7-*
5.9
86.7
100.0
ADJUSTED
FREQ
(PCT)
55.7.
44.3
MISSING
100.0
CUM
FRFO
(PCT)
55.7
100.0
100.0
VALID CASES
61
MISSING CASES 399
DP mMTjMlinijC i^a^TFVJ.ftTFP
CATEGORY LABEL
BATCH
! CONTUMU.Q11S _._
: _._R£LATIVE_-ADJUSTED - GUM-
ABSOLUTE FRE-Q FREQ FREQ
CODE FREO (PCT) (PCT) (PCT)
A
B
73
_.30
15.9
_ 6.5-
TOTAL
357
460
77.6
100.'b
VALID CASES
103
MISSING CASES 357
70.9 70.9
E9..1 :_. 1.0 Q»0—
MISSING 100.0
100.0
285 -
-------
03/21/7R
FILE - INK
- CREATED 03/21/78
0144
YEAR WASTEWATER TREATMENT SYSTEM WAS INS
RELATIVE
ABSOLUTE FPEQ
GORY LABEL CODE F'REQ (PCT)
56
57.
60
61
„. . . , . 62.
68
69
• 7ft
72
73
75
76
77
TOTAL
1
... 1
1
i
i
3
. 4
?
3
2
2
8
5
A
422
460
0.2
.. 0.2... .
'• 0.2 ^
0.2
. .. 0.2. -
0.7
0.9
0.4
0.7
0.4
ri.4
. 1.7
1.1
91.7
100.0
ADJUSTED CUM _
FREQ FREO
(PCT) (PCT)
2.6
2.6
•2.6
2.6
__. 2.6.-.
7.9
10.5
5^3
7.9
5.3
R-T
21.1
13.2
i n Q
MISSING
100.0
, 2.6
S,3
7.9
10.5
n?
21.1
31.6
Tft A
44.7
50.0
«?m •?
76.3
89.5
i nn n
100.0
VALID CASES
38
MISSING CASES 422
286
-------
03/21/78
FILE - INK
- CREATED 03/21/78
ABSOLUTE
CATEGORY LABEL CODE FREQ
.: so.
ion.
>. Voii:.
600,
i ' 700 .
1000.
1340:.
1500.
1800.
i 2000.
! iooo.
610S6.
10000.
i 1 1 o o o .
1117«.
15000.
1
j
i 17000.
- 18000.
20000.
acnnn
55000.
0.
;- • - : TOTAL
1
3
i
1
?
i
1
•?
1
3
i_
1
3
I
i
4
1
?
1
- i"
i
' 427
460
RELATIVE ADJUSTED
• FREQ FREQ
(PCT) ,(PCT)
' 0,2
0.2
0.2
0.4.
0.2
0.2
0.4
0.2
0.7
0.2
0.2
0.7
n . ?
0.2
0.9
0 .?
0.4
0.2
0.2
0.2
92.8
100.0
3.0
<3,1
3.0
3.0.
6^1. -
3.0
3.0
- ^«1
3.0
, 9.1
3.0 - -
. 3.0
9.1
- 3.0
3.0
12.1
3.0
6.1
3.0
3.0
3.0
MISSING
100.0
CUM.
FRFQ
(PCT)
3.0
12.1
15.2
18.2
24.2
27.3
30.3
36". 4
39.4
48.5
51 1*
54.5
63.6
66.7 .-'--..
69.7
81.8
84.8
90.9
93.9
97.0
100.0
100. 0
287
-------
03/25/78
S oiift
r
FILE - INK
AMMIIAL nprpftTjnM rncf15 nr
CREATED 03/21/78
G
ABSOLUTE
CATEGORY LABEL CODE FREQ
I
1
i
i
\
i
i
i
L . ...
i
10.
!
100.
150.
260.
600.
1000 .
3000.
9000.
0.
... , • ... TOTAL
1
I
.3
1
i
i
i
«
4
1
i'
435
.....460
ELATIVE
FREQ
-------
F:\_E -
- CREATED 03/21/73
Q149
SLUDGE STORED ON PLANT PROPERTY
CATEGORY LABEL
YES
ABSOLUTE
CODE FREQ
RELATIVE ADJUSTED
FREO FREQ
(PCT) (PCT)
A
TOTAL
..^458
460
0.4
99.6
100.0
100.0
MISSING
100.0
CUM
FRF.Q
(PCT)
100,0
100.0 .
VALID CASES"
MISSING CASES 458
......_. _.RELATIVE ADJUSTED CUM—
ABSOLUTE FPEQ FREQ FREQ
CATEGORY LABEL CODE FREQ (PCT)
[ YES ~B 3 0.7 100.0 100.0
L _ .:. .___ .452 : 99..3 -MISSING 10,0.0-.-
f~~ • -- - ' •- --. - 4»*»«»WM*» •»•••!••»«->« «•••«•••«•.••
TQTaL 460 100.0 . 100.0
VALID CASES 3 MISSIKIG CASES 457
; . • ' :
• ; - •' .--...••...".•' '
( \ ' "
>
V.-.-.Q1S1 SLUDGE IS SOLD
! . RELATIVE ADJUSTED CUM
i ' 'ABSOLUTE FREQ FREQ FRFQ
CATEGORY LABEL CODE FREQ (PCT) (PCT) (PCT)
I YES C -1?. 0.4 100.0 100.0
i .. .... ... ..'..... 458 99'.6 MISSING V100.0
! , . , -____„ ' -___„— ______
i TOTAL '. 460 100.0 100.0
VALID CASES
MISSING CASES
458
289
-------
03/21/78
FILE - INK
- CREATED 03/21/78
-SLUOGE—LS—CONIRACX-HlULED-
CUM
FRFQ
RELATIVE ADJUSTED
- ABSOLUTE FREQ FRFQ
CATEGORY LAPEL CODE FREO (PCT) (PCTJ
YES D 59 12.8 100.0 100.0
- , ------- . -- .... ________ ,_.. ________ &ni a?,? ____ MISSING— 100.0.
TOTAL 4-60 100.0 _. 10,0.0
VALID CASES 59 MISSING CASES 401
v._,Q153. ....... SLUDGE IS RECLAIMED
I RELATIVE ADJUSTED CUM
ABSOLUTE FPEO FREO FRFQ
CATEGORY LABEL CODE FREO (PCT) (PCT) , (PCT)
i 460 loo.o MISSING 100.0
j .,_ ...... , _ __ ..... ..TOTAL . ..46,0 ....... 100.0. .. 100.0 _____ . .
•._ VALID CASES. . o MISSING CASES 460 ..- . ...
(
I
S OLSA-
...SLUDfiE
CATEGORY LABEL
• RELATIVE.-.. ADJUSTED CUM_
ABSOLUTE FREQ FREQ FREQ
COOE FREQ (PCT) (PCT) (PC'D
TOTflL
9 2.0
.451 98.0
460 100.0
100.0 100.0-
MISSING- . .100.0..
100.0
VA.LID CASES
MISSING CASES 451
290
-------
; 03/21/7^ FILE - INK ' - CREATED 03/21/73
t * i ' •
i • . , • -
V—.Q.L56 I.5.. SLUDGE. .CQMQI TUNEo,
CATEGORY LAREL
YES, "
— NO . . _.._-_
: -. .RELATIVE- . ADJUSTED CUM-
!_ ABSOLUTE FREQ FREQ FREQ "
CODE FREQ (PCT) (PCT) (PCT)
3
J.15
0.7
-25 ..9-
2.5
TOTAL
33fl
460
73,5
100.0
2.5
_ SZ. 5_ _z
MISSING loo.o
100.0
VALID CASES:
122
MISSING CASES 338
V. Ql'57
CONTRACTOR USES PUBLIC LANDFILL
-._-.„„ ,„,
CATEGORY LABEL
YES
- ABSOLUTE
CODE FREO
50
410
-B^^-
460
RELATIVE ADJUSTED ... CUM
VALID CASES
50
TOTAL
MISSING CASES
FREQ
.(PCT)
10.9
S9.i
*-«•«»_.»
100.0
FREO
(PCT)
FREQ
(PCT)
100.0 100. Q"
MISSING, ._ 100.0....
•«>««.«.«
100.0
410
)=—JU53-
rnMTParTi-ip IJSES
- -
CATEGORY LABEL
YES
VALID CASES
ANDFILL
71
;_—,.,__ ------ ._-• ---- RELATIVE- ADJUSTED- -CUM
- ABSOLUTE FREQ FRFQ FRFQ
CODE FREO (PCT) (PCT)
-------
03/21/78
FILE - INK
- CRE&TED 03/21/73
Q159. CONIKAUIUK 1NUINC.WA 1 h.b 3LUUWC.
RELATIVE
ABSOLUTE
CATEGORY LABEL COPE FREQ
YES C 17
L .... ._ .. _443
TOTAL 460
VALID CASES 17 MISSING CASES 443
i
i
j
t _f
ABSOLUTE
CATEGORY LABEL CODE FREO
: "YES ° ?2
; 4-?*
| TOTAL 460
FREO
(PCT)
3.7
96.3.....
106.0"
ADJUSTED
FREQ
(PCT)
100.0
MISSING
100.0
?ELAT-I-V£ AOJUSZEO
FREO
(PCT)
4.8
<**,?
ioo.o
FREO
(PCT)
100.0
MISSXNG —
100.0
CUM .. ..
FREQ
(PCT)
•• — — •-
100.-0
1 OQ 0
*
^
-CUM. ' '..:
FREQ
(PCT)
100.0
.100.0
!.
1 VALID CASES 22 MISSING CASES 438
1 ' ' , '
I, CLL61 CONTRACTOR DISPOSAL METHOD UNKNOWN
t
i
l ABSOLUTE
} CATEGORY LABEL CODE FREO
! YES E 144
316
I • * * ~ «— •
TOTAL 460
RELATIVE
FREQ
(PCT)
31.3
68.7
100.0
ADJUSTED
FREQ
(PCT)
100.0
MISSING
100.0
CUM.. ....
FRFQ
(PCT)
100.0
100.0... ... ..
VALID CASES
144
MISSING CASES 316
292
-------
. FIUE -
- CREATED 03/21/78
Q163
COST PER GALLON OF SLUDGE DISPOSAL
RELATIVE ADJUSTED
; ABSOLUTE FREQ FRFQ
CATEGORY LABEL . COnE FREQ (PCT) {PCT>
- - . ' - ; . f .
. ' • " 2. : •-
3.
. - ••- ' - ---.- ... ., . .'. ' 4.-
,|' , ' ' . ' ' > ' "
____, . _„_..__
** i
. . . ' • '• . • 7._
9- :
- -11.
• : 12. i
IS;
" ' 17
^ ' - 18,. •
19,
----- -20^-
-
'.
4
.2
7
... .1
6
"""s ~-"T--
2_
2
4_
14
4
6.
6
2
|
1
1
- 1
1
^
0.9
0.4
1.5
0..2 -.
"Y.i """"" '
0.4
0.4
0.9
3.0
0.9
0.9
OA
1.3
0.4
n ?
0.2
0.2
0.2
-. )- -: L „* ..; •::,
0.2 •-
n . 7
0,9
0.4
1.5
. 0.2
.... i'3/ .,
1.1
-.0 ^4 .
0.4
0.9
0.9
0.9
.-O.A. ...
1.3
0.4
0.2
0.2
--0.7-
0.2
0.2
n 7
CUM
FREQ
-------
03/21/78 FILE - INK - C
zV
28.
32.
34.
47.
• "50.
i 69.
TOTAL
:REATEO
L.
2
1
7
1
1
1
1
1
1
460
33/21/78
0*9
0.4
0.2
1.5
0.2
0.2
n.7
0.2
0.2
.0.2
100.0
0 Q
0.4
0.2
i
•- .liS ...
0.2
0.2
r>,7
p. 2
0.2
0.2
0.2
100.0
96.3
96.5
98.3
98.5
pq.l
99.3
99.6
100.0
294
-------
Q3/21/7A FILE - INK ,, -CREATED 03/?1X78
Q164 PERCENT OF FLOW BECOMING SLUDGE .,
CATEGORY LABEL
0 TO 5
6 TO 10
11 TO 15
ABSOLUTE
CODE FREQ
A 40
8 8
C 9
TOTAL
404
'+60
RELATIVE ADJUSTED
FREQ FREQ
(PCT> (PCT)
8.7 71.4
1.7.. . 14.3 . .
1.7 ' 14.3
87.8 MISSING
CUM
. FREQ
(PCT)
71.4
... 85.7 .
100.0
100.0
100.0 .„._, 100.0 _..
VALID CASES
56
OFFSPFC
MISSING CASES 404
uTTH
CATEGORY LABEL
YES " "'
—— —RELATIVE—ADJUSTED CUM _
ABSOLUTE FREQ FREQ FRFQ"
CODE FREO (PCT) (PCT) (PCT)
TOTAL
460
0.7 100.0 r 100.0
_..9.9 ^3^ MISSING 100.0—
100.0 100.0
VALID CASES
MISSING CASES 457
S-..-Q166.
OFFSPEC INK SOLD TO SCAVENGERS
CATEGORY LABEL
YES'1
VALID CASES
42
RELATIVE ADJUSTED CUM
ABSOLUTE FREQ FREQ ' FRFQ
CODE FREQ (PCT) (PCT')
,B
TOTAL"
MISSING CASES
42
41fl
460
SES '" 418
:95 -•
• 9.1
90.9
100.0
100.0
MISSING
100.0
100.0
100.0
;
-------
03/31/78
FILE - INK
- CREATED 03/21/78
C.ATEGORY LABEL CODE
' YES C ,
TOTAL
t
t
VALID CASES 85 MISSING
}
ABSOLUTE
85
460
CASES 375
1
V.. .Q168_ OFFSPEC INK BLENOF.D INTO OTHER PRO
ABSOLUTE
CATEGORY LABEL CODE FREQ
YES . D 378
8?
TOTAL
VALID CASES 378 MISSING
460
CASES 82
RELATIVE
FREQ
(PCT)
18.5
100.0
DUCT
RELATIVE
FREQ
((PCT)
82.2
1.7.8
100.0
ADJUSTED
FREQ
(PCT)
100.0
MISSING.
100.0
ADJUSTED
FREQ
(PCT)
* lOO'.O""
MISSING
100.0
CUM ..
FRFQ
(PCT)
100.0
100.0
CUM .
FRFQ
(PCT)
100.0
100,0
-QE-
CATEGORY LABEL
_, . RELATIVE:. ADJUSTED ... CUM...
ABSOLUTE FREQ FREQ FRFQ
CODE FREQ (PCT) (PCT) (PCT)
.GIVE
• HAUL
PAY
TOTAL -
1 '
1_
1
457
460
0.2
0 , 7>
0.2
99.3
. 100.0.
33.3 33.3
_33.3 66.7
33.3 100.0
100.0
MISSINO
.100.0 .. -. -...
•_..VALID CASES.
, 3. MISSING CASES '...457..— ..
296
-------
<33/21/7fl FILF - INK , - CREATED 03/21/78
. " - - V
Q170 PLANT HAS PH ANALYSIS OF WASTEWATF.P
CATEGORY LABEL
RELATIVE ADJUSTED CUM
ABSOLUTE • FRF.Q FREO FRFQ
CODE FREO (PCT) (PCT) (PCT)
i Tt5 , _ . A 53 11.5
-407 88.5
TOTAL K 460 100.0
VALID CASES 53 MISSING; CASES 407
^ °i7i PL«MT HA.S ROD AMAL.YSTS OF WASTEWATF°
.. _....," ..'.', RELATIVE
- • ; ABSOLUTE FREQ
CATEGORY, LARFL COHE FREQ (PCT)
YES B 33 7.2
•*
TOTAL 460 100.0
/ VALID CASES 33 MISSING CASES 427
i - 'A
,r --:-— - .
i • - ' • - •'• •.'.-••'
^ — 0172. :......_. PLANT HAS COD ANALYSTS OF WASTEWATER
RELATIVE
„ „ • ' ' ABSOLUTE FREQ
CATEGORY LABEL , CODE FREQ (PCT) -
'vc ' ' '" '' "' •
ES C Ifl . 3.9
442 96.1
. • •. TOTaL 460 100.0
100.0 100.0
MISSING ioo.o.._..
loo.q
AO.JUSTFP CtIM
FREQ FRFQ
(PCT) (PCT)
100.0 100.0
MfSSINfi 100 0
100.0
ADJUSTED CUM
FREQ FRFQ
(PCT) (PCT)
100.0 100.0
MISSING loo.o
100.0
VALID CASES
IS
CASES 442
297
-------
03/21/78
FILE - INK
-•"CREATED 03/21/78
7T
!
j CATEGORY LABEL
~~~YES
CODE
D
ABSOLUTE
FREQ
RELATIVE
FREQ
(PCT)
TOTAL
32 7,0
...428 -9.3 ..0—
460 100.0
ADJUSTED
FREQ
(PCT)
100.0
-MISSING—
100.0
CUM
FRFQ
(PCT)
100.0
JL O0.^0_.
VALID CASES
32
MISSING' CASES 428
.. Q1Z4. PLANT HAS TOTAL SOLIDS AMALSIS OF WASTEW
CATEGORY LABEL
YES
CODE
E
..._._.,.
TOTAL
' RELATIVE ADJUSTED CUM...
ABSOLUTE FREQ FREQ FREQ
FREQ (PCT)
-------
FILE - INK
- CREATFD 03/?l/79
Q176
PLANT HAS OIL AND GRFASE, ANALYSIS
CATEGORY LABEL
RELATIVE ADJUSTED CUM
ABSOLUTE FREQ FREQ FREQ
CODE FREQ (PCT) (PCT) (PCT)
.
•
,-
•
_
..
••
I
:
1
YES G 17
: 443
3.7
96.3
.- ' TOTAL 460 100.0
VALID CASES 17/ MISSING CASES 443
tti77 PLANT HAS Ti"5siniTY ANALYSIS o^ '-"V^TEWAT
RPI ATTUF
ABSOLUTE
CATEGORY LABEL CODE FREQ
YES, H 5
•
TOTAL 460
VALID CASES 5 MlsSIMG CASES 455
.- ' .._...,...._:
. _QL78 ._ PLANT HAS TRACE ORGANJICS ANALYSIS
' ABSOLUTE
CATEGORY LABEL CODE FREQ
YES . • I 5
' ' 455
, TOTAL 460
VALID CASES ; 5 wlSSI'NG CASES 455
FREQ
(PCT)
!•!
100.0
RELATIVE
. .FREQ
(PCT)
'l.l
98.9
100.0
100.0
MISSING
100.0
ADJUSTED- -
FREQ
(PCT)
100.0
MISSING '-
100.0
ADJUSTED
FREQ
(PCT)
100.0
MISSING
100.0
JOO.O
100.0 :
-
\
. CUM
FRFQ
(PCT)
100.0
1*00.0
.
CUM
FRFQ
(PCT)
100.0
100.0 "
-------
03/21/78
FILE - INK
- CREATED 03/23/78
Q180
NEW CAP COST FOR RASFLINE WATER POLL REG
| CATEGORY LARF.L cOr>E
500.
-. .. . • :J32.06.
i 4000.
5000.
- — ..-- 6000..
« 7500.
10000.
}••- - _J_9.0fto.
! 15000.
i
200,0.0..-.
IT — — "SO-OiL.
30000.
38000.
_.__ — . _ _ .400Qfl~.
j 50000.
! 60065.
. .8.0.00-0-.
125000.
150000.
— — --- 1^5-0-dn
1500000.
0.
i _ — . XQZ4L
RELATIVE ADJUSTED
ABSOLUTE FREQ FREQ
FREQ (PCT) (PCT.
1
' 1.
1
2
1
1
11
1
2
4-
3
3
1
j
2
2
1
1
1
i"
1
: . *18'
4fin
0.2
0.2
0.2
0.4
...O.2.
0.2
2.4
0.?
0.4
0.9
n .7
0.7
0.2
-.. .... -0.2.
0.4
0.4
a^
0.2
• 0.2
A O
U-«-C —
0.2
90.9
1 rt rt ft
__| UU • U —
2.4,
2.4...
2.4.
4.8
2.4
2.4
26.2
?. h.
4.3
9.5
7 1
7.1
' 2.4
,4
4.8
4.8
o /.
2.4
-2.4
2 « .4
2-4
MISSING
1-00.. 0
CUM
FRFQ
,
-------
03/21/7S
FILE - INK
- CREATED Q3/21/7B
CATEGORY LA8FL COOE
o.
.... . 175.
'...-.: -.'son;.
700!.
-V..' , ... 800.
Tooo.
1200.
150 0«
1831.
. ?ooa.
3000.
3500.
4000.
4500.
.'.... . 5000.
'
'
9000.
, 12000.
20000.
, ' 135000.
. ...''_ ...TOTAL
ABSOLUTE
FREQ
409
i
. _ 1
8
1
1
5
i
3
2
S •
1
5
3 •
1
3
•p
1
. i
460
RELATIVE t
FREQ
(PCT)
88.9
0.2
0.4
0.2
,0.2..—,-.
1.7
0.2
0.7
. 0.2
i .i
0.2
JO-.7
0.4
1 » 1
0.2
'i.i
0.7
0.2
,-0,7
0.4
0.2
0.2
100.0
iOJUSTE
FREQ
(PCT)
88.9
0.2
0.4
0.2
0.2
1.7
0.2
..1.0.7
0.2
l.'l
0.2-
0.7
0.4
1.1-
0.2
1.1
0.2
0.7
.- -0..4-
0.2
0.2
100..0
D CUM
FREQ
(PCT)
88.9 -
89.6
89.8
.90.0
91.7
92.0
92'. 8
93.9
04 . 1
94.8
95.2
96.5 ,
97.6
98.3
98.5
99.1
9Q 6
99.8
100.0
301
-------
03/21/78
fILF. - INK
- CREATED 03/21/78
Q182.
ODOR REGS TO HAVE ECONOMIC IMPACT ON P[_A
CATEGORY LABEL
YES
VALID CASES
i
_DJ-S3
RELATIVE' ADJUSTED CUM
ABSOLUTE FREQ x FREQ FREQ
CODE FREQ (PCT) (PCT) (PCT)
. .... 45L
TOTAL 460
MISSING CASES 451
2.0 100.0 100.0
. , 98.0- MISSING ... 100...0-
100.0 100.0
IMpAT
r
CATEGORY LABEL
: BELATI-VE ADJUSTED CUM-
ABSOLUTE FPEQ FREQ FREQ
CODE FREQ (PCT) (PCT) (PCT)
YES 8
.TOTAL
5
460
1.1 100.0
.100.0 100.0
100.0
i f i n . n
VALID CASES
MISSING CASES 455
1
L
.018,4 SOLID WASTE REGS TO HAVE ECONOMIC IMPACT
CATEGORY LABEL
YES
RELATIVE ADJUSTED ' CUM .
ABSOLUTE FREQ FREQ FRFQ
CODE FREO (PCT) (PCT) (PCT)
C 59 1?.8 100.0 100.0
. ..... .401 87.2 MISSING 100.0-
TOTAL 460 100.0 100.0
VALID CASES
59
MISSING CASES 401
302
-------
03/21/7P
FILET - INK
- CREATED 03/21/78
=—0135 __-
1SHA..J3EGS.-..T.O HA VE_£CnNO.M IC-IMPAC
CATEGORY LABEL
YES ; "
' •• RELATIVE ADJUSTED . CUM
ABSOLUTE FREO FRFQ FRFQ
CODE FREO (PCT) '(PCT) (PCT)
110 23.9 100.0 100.0
—MISSING— 100.0._.
100.0
VALID CASES
110
TOTAL 460 100.0
MISSING CASES 350
V Q186
AIR POLL CONTROL PEGS TO HAVE IMPACT
CATEGORY LABEL
YES
VALID CASES
46
RELATIVE ADJUSTED CUM
ABSOLUTE FREO FRF.Q FRFQ
CODE FREO (PCT) (PCT) .(PCT)
TOTAL
46
414
460
10.0
90.0
.100.0
MISSING CASES- 414
100.0
MISSING
100.0
100.0
IOQ.Q
HAVF
n\) PLANT
CATEGORY LABEL
VALID CASES
67
_ __.. ....RELATIVE-. AD JUSTED CUM.
- ABSOLUTE FREQ FREQ FREQ
CODE FREO (PCT) (PCT) (PCT)
F .67 14.6
'w ,.,.393.. .85.4.
TOTAL 460 100.0
100.0 100.0
.MISSING 100.0..
100.0
MISSING CASES 3<53
303
-------
03/S1/73
FILE - INK
-CREATED 03/21/78
Qiaa
SAFE DRINKIMG WATFR ACT TO HAVE IMPACT
i CATEGORY LABEL
1
YES
RELATIVE ADJUSTED
ABSOLUTE FREQ FREQ
CODE FREO (PCT)
-------
03/21/78
FILE - TNK
- CREATED 03/21/78
V--Q-1-89-
-MEW.-CAP- COSTS .JO-MEET.-ALL—REG-,-AR£AS—.
CATEGORY LABEL
ABSOLUTE
COnE FREO
RELATIVE
FRFQ
(PCT)
ADJUSTED
FREQ
(PCT)
CUM
FRFQ
(PCT)
305
-------
03/P1/78
FILE - INK
- CREATED 03/21/78
90000.
100000.
1
; .125000.
!
150000.
pooooo.
250000.
300000.
4.00000.
500000.
i
1 _
6.
TOTAL
f, ^
1
r
1 !'
I
1 0.2 0.9 ..89. a.
3 0.7 2.8 91.7
' f 0.2 , 0.9" 92.7 "
1 0.2 0.9 93.6 ...
2 0.4 1.8 95.4
1 0.2 0.9 96.3
1 6.2 0.9 _97.2. — ._
1 0.2 0.9 98.2
1 0.2 0.9 99.1
£ 0*2 0.9 10 0.0
351 76.3 MISSING 100.0
1 ^ ,—
460 100.0 100.0
306
-------
03/21/78
FILE - TNK
- CREATED 03/21/78
"I
v — 04,9.0-
-AWWUAL-.OPER.-COST.S-TO .M££T -4LL-.REG-JiR.E4S.
CATEGORY LAPEL COHE
: ion.
ISO
250.
500.
— --' — fono. .
1200.
. 1500 i,
''flon
*
~ •• : ?5oo.
?700.
T o o o
• *
4000i
5000.
fioori
"
ftion.
., ,
7000.
'~- ; -•- ' 7200.
7500.
P 0 0 0 .
.
P500.
looon.
1?000.
•-- 15000.
ABSOLUTE
1
1
1
*
.. g
l"
2
i n
1
1
4
1
6
•5-7
1
2
1
1
3
1
3
2
4
RELATIVE t
FREO
(PCT)
0.2
0,2
0.2
0.9
U7
0.2
0.4
? 2
0.2
0.2
OQ
0.2
1.3
0.2
0.4
0.2
0.2
0.7
0.2
0.7
0.4
0.9
lOJUSTFO
FREQ
(PCT)
0.9
fl Q
0,9
3.6
... -7.3---.
0.9
1.3
91
..i .. —
0.9
0.9
3gL
• o
0.9
5.5
33.6 •
0.9
1.8
0.9
0.9
2.7
0.9
2.7
1.8
3.6
CUM
FRFQ
(PCT)
0.9
1 Q
2.7
6.4
13. -6
14.5
16.4
25*5
26.4
27.3
30 .9 . ,
31.8
37.3
70.9
71.8
73.6
74.5
75.5
78.2
79.1
81.8
83.6
87.3
307
-------
03/21/7B
FILE -
- CRE&TEO 03/21/78
19000.
19500.
20000.
30000.
37500.
47000.
60000.
65000.
1050,00.
148000.
0.
TOTAL
1
1
3
2
1
' ?
i
i
i
i...
350
460
0.2
0.2
0.7
0.4
0.2
0.4
0.2
0.2
0.2
0.2
76.1 k
100.0
0.9
0..9
2.7
i.a
0.9
1.8
0.9
0.9
0.9
0.9 ...
100«0
88.2
89.1
91. 8
93.6
94..S
96.4
97.3
98.2
99.1
.1.00..Q
-100.0
308
-------
03/21/78 FILE - INK
-RM.1.
-WJ=LI..I£_LEAD--.P.IGMF.NT._
- CREATED 01/21/78
CATEGORY LABEL
NO. PLANTS IJSIMG
VALID CASES
RELATIVE ADJUSTED CUM.
ABSOLUTE FREQ F'RFQ FRFQ
CODE FREO
-------
03/21/78
FILF - INK
- -CREATED 03/21/78
RM4
ABSOLUTE
CATEGORY LAREL CODE FREO
NO. PLANTS USING D is
"... , ._44S
TOTAL 460
I
VALID CASES 15 MISSING CASES 445
i
I OM =
f
ABSOLUTE
CATEGORY LABEL COHE FREQ .
NO. PLANTS USING £ ' 5?
•
TOTAL 460
VALID CASES 5-2 MISSING CASES 408
f
V,»_RM6 , ZINC YELLOW
~" ABSOLUTE
CATEGORY LABEL CODE FREO
| NO. PLANTS USING F 2
..... 458
' TOTAL 460
RELATIVE
FPEQ
(PCT)
3.3
96.7
100.0
PCI ATTVF
FREQ
(PCT)
11.3
Rfl ,7
100.0
RELATIVE
FRF.Q
(PCT)
0.4
99.6
100,0
ADJUSTED
FREQ
(PCT)
100.0
MISSING-
100.0
CUM
FREQ
(PCT)
100.0
100«-Q ..
_AO lu^TFn n IM
FREQ FPFQ
(PCT) (PCT)
100.0
- s -L 3--
100.0
ADJUSTED
FREQ
(PCT)
100.0
MISSING
100.0
100.0
i no ft
CUM ..
FREQ
(PCT)
100.0
10 O.Q.._
VALID CASES
MISSING CASES 4-58 .
310
-------
FILE - INK
- CREATED 03/21/78
CATEGORY LABEL
... R£LA±I.VE—A.O JUSIED C1JM_
ABSOLUTE FREQ FREQ FRfQ
CODE FREQ (PCT) (PCT) (PCT)
NO. PLANTS USING
0.7
qg.3
100.0
MTS.SJJ
100.0
100.0
TOTAL
460
100.0
100.0
MISSING CASES 457
\> RMS
-MISC MI AG CU PB-OR BRONZE
CATEGORY LABEL
NO. PLANTS USING
,-: RELATIVE... ADJUSTED CUM_
ABSOLUTE FREQ FREQ FREQ
CODE FREQ (PCT) (PCT) (PcT)
H
268
_L22_
TOTAL
460
58.3 100.0
—4i.»7. MISS INC
100.0 100.0
100.0
_LO.a_Q
VALID CASES
268
MISSING CASES 192
• DC1! A TT WC1
ABSOLUTE FREQ
CATEGORY LABEL CODE FREQ (PCT)
NO. PLANTS USING I 79 17<2
• "5 Si ars a
TOTAL 460 100.0
— AOJ.US1ED-
FREQ
(PCT)
100.0
M T QC TMr*
100.0
FRFQ
(PCT)
100.0
VALID CASES 79 MISSING CASES 381
311
-------
03/21/78
FILE - IMK
- CREATED 03/21/78
.. RM1Q CADMIUM
CATEGORY LABEL
NO. PLANTS USING
'. VALID CASES 50
PMJl TWOOMF fSP££M
CATEGORY LABEL
NO. PLANTS USING
I VALID CASES 24
k. RM1 ? CHROMIUM OXtDF
•CATEGORY LABEL
NO. PLANTS USING
1
f ' " "
i
RELATIVE
ABSOLUTE FREQ
COnE FREO (PCT)
J 50 10.9
-^All).. , ._ 89. !,._
TOTAL 460 100.0
MISSING CASES 410
PFLA-T-I-U£
ABSOLUTE FREQ
CODE FREQ
-------
03/21/78
FILE - IMK
- CREATED 03/21/78
i BM4-3-
I CATEGORY LABFL '
NO. PLANTS USING
VALID CASES
• - —RELATIVE. ADJUSTED. CUM .
ABSOLUTE FREQ FRFQ FREQ
CODE FREQ (PCT) (PCT) (PCT)
M
TOTAL
2.0
460
100.0
MISSING CASES 451
100.0 100.0
-MISSING 10Q.-Q—
100.0
CADMIUM YELLOW OR ORANGE
CATEGORY LABEL
RELATIVE ADJUSTED CUM_
ABSOLUTE FREQ FREQ FRFQ
CODE rREQ (PCT) (PCT) (PCT)
| NO. PLANTS USING A ; 64 13.9 1QO.O "lOO.V
•-— -• : - •'••- -.--.. —396 . —-,86.1 MISSING 10Q..Q_
I . . _' "~ —™—~ --.—-- --._,„-«
1 TOT4L 460 100.0 100.0
VALID CASES 64 MISSING CASES 396
i
I
S RM.iq rMPOMF vc'LLni-ir
1 --.,,..._.RELATIVE -ADJUSTED— CUM__
4RSOLUTE FREQ FREO FRFO
CATEGORY LABEL COnE FREQ (PCT) (PCT) (PCT)
NO. PLANTS~USING"" a" "322 "TO'.O ioo."o iob"."o"~
j _ :. ,..i; ; .__i3a 30<§o .MISSING . 100.0..
TOTAL 460 100.0 100.0
VALID CASES 322
MISSING CASES
313
138
-------
03/21/7B
FILE -
- CREATED 03/21/78'
RM16.. ,
CHROME ORANGE
CATEGORY LABEL
NO. PLANTS USING
VALID CASES
24
RELATIVE ADJUSTED CUM
ABSOLUTE FREQ FREQ FRFQ
CODE FREQ (PCT) (PCT)
100.0
TOTAL
MISSING CASES 436
24
436
460
5.2
... .94.8
100.0
100.0
MISSING
100.0
CATEGORY LABEL
RELATIVE—ADJUSTED - CUl-
ABSOLUTE FREQ FREO FRFQ
COnE FREQ JPCT) (PCT> (PCT)
NO. PLANTS USING o
i
! TOTAL
307
460
66.7
33. T
ioo.o
100.0
100.0
100.0
10". 0
VALID CASES
307
MISSING CASES 153
•v JRHiQ .-..LEAD
CATEGORY LAP.EL
NO. PLANTS USING
RELATIVE ADJUSTED
ABSOLUTE FREQ FREQ
CODE FREQ (PCT) (PCT)
TOTAL
CUM ______
454
460
1.3
98.7
100.0
100.0
MISSING
100.0
100.0
100.0
VALID CASES
MISSING CASFS
454
314
-------
03/21/78
FILE - INK
- CREATED 03/21/78
.PHLOXJNE_#E0
!
I CATEGORY LABEL
! ; _
: NO. PLANTS USING
RELATIVE. ADJUSTED CUM ..
ABSOLUTE FREQ FREQ FRFQ
CODE FREO (PCT) (PCT) (PCT)
129
28.0
100.0
100.0
VALID CASES
129
>.-_RM20.~ . -. LEAD
TOTaL
460
100.0
100.0
MISSING CASES 331
CATEGORY LABEL
NO. PLANTS USING
VALID CASES
RELATIVE ADJUSTED CUM .
ABSOLUTE FREO ' FREQ FREQ
CODE FREO (PCT) (PCT) (PCT)
TOTAL
MISSING CASES 4-57
3
457
460
0.7
.... 99.3
100.0
100.0
MISSING
100.0
100.0
100.0 _....
CATEGORY LABEL
NO. PLANTS USING
VALID CASES
57
..._ _._-RELATIVE ADJUSTED CUM
ABSOLUTE FREQ FREQ FREQ
CODE FREO (PCT) (PCT) (P.CT)
TOTAL
MISSING CASES
57 12.4 100.0 100.0
.403 87.6 .. MISSING. .. 100.0
460 lOO.O 100.0
403
315
-------
03/21/73
FILE - INK
- CREATED 03/21/78
RM22
IRON BLUE WITH CYANIDES
| CATEGORY LABEL
t
'. NO. PLANTS USING
VALID CASES 299
v — RjA?*v ?TM^ no rnPOMT
* *„.* i
[ CATEGORY LABEL
1 NO. PLANTS 'USING ••-•
L. . . ._ ... ... ,.,. ... •
VALID CASES 1
i
V, — RM2.4, . . PHTHALOCYANINE
'"
CATEGORY LA.BEL
NO. PLANTS USING
VALID CASES 343
CODE
I
TOTAL
MISSING
Lj.M_aaoutii-
COOE
J
TOTAL
MISSING
BLUE
CODE
K
TOTAL
MISSING
ABSOLUTE
FREQ
299
161
RELATIVE
FREQ
(PCT)
65.0
- 35.0
460 100.0
CASES 161
ABSOLUTE
FREQ
1
460
CASES 459
ABSOLUTE
FREQ
343
117
460
CASES 117
DCI ATTWp
FREQ
(PCT)
0.2
QQ ft
100.0
RELATIVE
FREQ
(PCT)
74.6
25.4
100.0
ADJUSTED
FREQ
(PCT)
100.0
MISSING
ioo.o
AH ii iCTcrn
FREQ
(PCT)
100.0
M T <^QT Ml^
100.0
ADJUSTED
FREQ
(PCT)
100.0
MISSING
100.0
CUM
FRFQ
(PCT)
100.0
100.0 . -..
f*i IM
FRFQ
(PCT)
100.0
IA n f\
CUM
FRFQ
(PCT)
100.0'
100.0
316
-------
03/21/7R
FILE - IN*
- CREATED 03/21/78
-R.M25-
CATEGORY LABEL
MO. PLANTS USING
CODE
L
TOTAL
RELATIVE ADJUSTED.. . CUM_
ABSOLUTE FREQ FREQ FRFO
FREQ .(PCT) (PCT) (PCT)
32? 70.0 100.0 100.0
-L3S 30.0 MISS ING 10 0* 0_
460 100.0 100.0
VALID CASES
322
MISSING CASES 138
RM26
... CHROMIUM PIGMENTS
CATEGORY LABEL
VALID CASES.
__^__.-.- RELATIVE ADJUSTED . _. CUM_
.,— ABSOLUTE FREO FREQ FREQ
COOE FREO (PCT) (PCT) (PCT)
-TOTAL
460
««M«D4WW«
...460
100.0
100.0
MISSING
100.0 .
100.0
MISSING CASES A60
PM77
CATEGORY LABEL
NO. PLANTS USING
'__.._ RELATIVE ADJUSTED GUM-
ABSOLUTE FREQ FREQ FREQ
COHE FREQ (PCT) (PCT) (PCT)
N
TOTAL
1 -0.2 100.0 100.0
_459 9.9 . 3 MISSING 100.0-
460 100.0 100.0
VALID CASES
MISSING CASES 459
317
-------
03/21/73
PILE - INK
- CREATED 03/21/78
RM28
LEAD PIGMENTS
ABSOLUTE
CATEGORY LAREL CODE FREQ
I
460
„-.-..; -, TOTAL 46Q
•
VALID CASES o "ISSIMG CASFS 4&o
L PMPQ
i
i
! .
RELATIVE
FREQ
(PCT)
100.0
100.0
TQMFD
CJFI ATTVF
! . ABSOLUTE FRFQ
| CATEGORY LABEL . CODE FREQ
NO. PLANTS USING P 204
•
?^A
TOTAL 460
.
•VALID CASES 204 MISSING CASES 256
t
i
i • .
v. RM30 DICHLOROBENZIDENE DlARYLIDE YFLLOW
i
I • ABSOLUTE
i CATEGORY LABEL COOE FREO
I
J
NO. PLANTS USING A 31*
;. . . ..... 142
j TOTAL 460
((PCT)
44 ..3
5=5.7
ioo.o
TONER
RELATIVE
FREQ
(PCT)
69.1
30.9
100.0
ADJUSTED
FREQ
(PCT)
MISSING
100.0
...
ADJUSTED
FREQ
(PCT)
100.0
MISSING
100.0
ADJUSTED
FREQ
(PCT)
100.0
MISSING
100.0
CUM
FRFQ
' (PCT)
-...
100.0
f*t !M
FRFQ
(PCT)
100.0
inn n
CUM .... ....
FRFQ
(PCT)
100.0 •
100.0.
VALID CASES
318
MISSIMG CASES
142
318
-------
_r
03/21/78
FILE - INK
- CREATED 03/?l/78
PYRAZOLOMF—RE-D
i ABSOLUTE
CATEGORY LABEL COOE FREQ
i NO. PLANTS USING B 55
-. - — - - - . .-...- _ .. 4.QS-
TOTAL 460
RELATIVE.
FRFQ
(PCT)
12.0
100.0
ADJUSTED-
FREQ
• (PCT)
100.0
MISSING
100.0
CUM
(PCT)
100.0
100 0
VALID CASES
55
MISSING CASES 405
V -RM32 ,._. MISC RED WITH ZINCtCR, OR PB
CATEGORY LAREL
NO. PLANTS USING
VALID CASES
49
RELATIVE ADJUSTED- CUM...
ABSOLUTE FREQ • FREQ ' FRFQ
CODE FREQ (PCT) (PCT) (PCT)
49
TOTAL
460
10.7 100.0 100.0
. 89.3 . MISSING..-.. 100.0.
100.0 100.0
MISSING CASES 4ii
YFLLOW WITH ANITTMONY OP CHPQMIIJM
CATEGORY LABEL
i VALID CASES
I .... _
41
-.-RELATIVE- ADJUSTED- CUM-
ABSOLUTE FRFQ FREQ FRFQ
CODE FREQ '(PCT) (PCT) (PCT)
USING
D
'
TOTAL
41
419
460
8.9
91.1
100. 0
100.0
MISSING
100.0
100.0
100.0
MISSING CASES 419
319
-------
03/21/7H
FILE -
- CREATED OV21/78
CATEGORY LABEL COQE
NO. PLANTS USING E
TOTAL
VALID CASES 18, MISSING
v, DM^C; MJSP VFLLQV/ WITH MICKFL
i
i" '" - '
; CATEGORY LABEL COOE
I
NO. PLANTS USING F
I
i
j TOTAL
! VALID CASES 3 wlssiWG
i
t
i
i
C RM3.6 MISC CHROMIUM SLUFv
jt
8_ f
*
CATEGORY LABEL COnE
i NO, PLANTS USING G
i TOTAL
RELATIVE
ABSOLUTE FREQ
FREO (PCT)
18 3.9
......442... . 96.1_._.
460
CASES 442
ABSOLUTE
FREQ
3
&=;?
460
CASES 457
ABSOLUTE
FREO
2
.. 458
460
100.0
ADJUSTED
FRFQ
(PCT)
100.0
MISSING—
100.0
RELATIVE — ADJUSTED -
FREQ FREQ
(PCT) (PCT)
0,7
QQ.3
100.0
RELATIVE
FREQ
(PCT)
0.4
99.6
100.0
100.0
-MISS-LbJG
100.0
ADJUSTED
FREQ
(PCT)
100.0
MISSING
100.0
CUM
FRFQ
(PCT)
100.0
100.0
CUM
FRFQ
(PCT)
100.0
}nn.n
CUM
FRFQ
(PCT)
100.0
100.0 . ._. _
VALID CASES
MISSING CASES 458
320
-------
—SM3-7—
FILE - INK-
JAISC.~CADMJJJM.. BLUES
- CREATED 03/21/78
CATEGORY LABEL
NO. PLANTS USING
RELATIVE. ADJUSTED. CUM-
ABSOLUTE FREQ FREQ FRFQ
CODE FREQ (PCT) (PCT) (PCT)
H ;?
TOTAL 460
0,4
QQ.A
100.0
100.0
100.0
100.0
1 0 0 • 0
VALID CASES
MISSING CASES 458
1
V-..RM38.. . .. MISC COPPER BLACK
:i •
CATEGORY LABEL
NO. PLANTS USING
•-.-•-.. RELATIVE ADJUSTED . CIJM_
ABSOLUTE FREQ FREQ FREQ
CODE FREQ (PCT) (PCT) (PCT)
VALID CASES
TOTAL
460
0.9
100.0
100.0 100.0
MISSING ]
100.0
MISSING CASES 456
L
1
L.
MTcr
CATEGORY LABEL
RELATIVE-—ADJUSTED - .GUM-
ABSOLUTE FREQ FREQ FREQ
CODE FREQ (PCT) (PCT) (PCT)
._TOTiL.-
460
-46.Q-.
100.0
_LO 0 ...Q
MISSING loo.o
-VALID. CASES ...0..
.MiSSlAlG -CASES 46A.
321
-------
03/21/7*
FILE - INK
- CREATED D3/21/7R
RM4Q
MISC ANTIMONY LEAD OR ZINC YELLOW
CATEGORY LABEL
NO. PLANTS USING
wrr i.
CODE
K
. — ..
OTAL
ABSOLUTE
FREQ
41
.....417.
460
RELATIVE
FREQ
(PCT?
9.3
90.7
100.0
ADJUSTED
FREQ
(PCT)
100.0
MISSING ..
100.0
CUM
FRFQ
(Pr.T)
100.0
100.0
•VALID CASES
43
MISSING CASES 417
57M
flNTTMQNY WHITE ^OUFO'J*
CATEGORY LABEL
NO.'PLANTS USING
RELATIVE ADJUSTED GUM-
ABSOLUTE FREQ FRFQ FREQ
CODE FREQ (PCT) (PCT) (PCT)
TOTAL
460
0.2 100.0 100.0
__99 .3 M.I SSIN6 1 0 0 »0-
100.0 100.0
VALID CASES
MISSING CASES 459
. RM4a__
DICHLOROBENZIDENE RED AQ
CATEGORY LABEL
NO, PLANTS USING
RELATIVE ADJUSTED
ABSOLUTE FREQ FREQ
CODE FREQ (PCT) (PCT)
M
TOTAL
28
432
460
6.1
93.9
100.0
100.0
MISSING
100.0
CUM
FRFQ
(PCT)
100.0
100.0
VALID CASES
28
MISSING CASES 432
322
-------
03/21/70
FILE - INK
- CREATED -03/21/78
CATEGORY LABEL
RELATIVE ADJUSTED
ABSOLUTE FREQ F~REQ
CODE FREQ (PCT) (PCT)
JSING . N
• TOTAL
90
^70
460
19.6
80.4
100.0
100.0
MT SM4S-
nff
CATEGORY LABEL
NO. PLANTS USING '
VALID CASES
88
.RELATIVE ADJUSTED .. CUM._
ABSOLUTE FREQ FREQ FREQ
CODE FREO (P.CT) - (PCT) (PCT)
TOTAL
2
458
460
0.4 . 100.0' I'OO.O
99.6 MISSING .. 100.0.
100.0 100.0
MTSSIMG CASES 458
AO
.,^__-—.--. ,.,.._ .,;.__•.£. EL A TIVE -ADJUSTED- CUM...
ABSOLUTE FREQ FREQ FREQ
- COOE FREQ (PCT) (PCT) (PCT)
..--.-. ...-•_^_._ 372 .1.
T.OTaL 460
19.1 100.0 ,100.0
SO.9 — MISSING- - 100.0
10-0..0 100.0
MISSING CASES 372
323
-------
03/21/7S
FILE - INK
- CREATED 03/21/78
RM46
NICKEL OR CADMIUM YEl LOW AQ
CATEGORY LABEL
RELATIVE ADJUSTED
ABSOLUTE ' FREO FRED
CODE FREO (PCT) __RiU
ORANGE LEAD ftQ-
i
I CATEGORY LABEL
I _«__ ,IT- '
* NO."PLANTS-USING
RELATIVE ADJUSTED CUM-
-ABSOLUTE FREO FREQ - FR*EQ
COriE' FREO (PCT) (PCT) (PCT)
TOTAL
61 13,. 3 100.0 • 100.0
__3.93. 86,. 2 MISSING—1 00 ..0.
460 " 100.0 lOOoO :'
VALID CASES
61
MISSING CASES 399
I
V ,.RM48... ._ . DICLOROBENZIDENE.ORAMGE AQ
CATEGORY LABEL
VALID CASES
RELATIVE ADJUSTED CUM .
ABSOLUTE -FREQ FREO FRFQ
CODE FREO (PCT) (PCT) l-PCT)
TOT4L
3
457
mmm^^m
460
MISSING CASES
0.7
99.3
100.0
100.0
MISSING
100.0
100.0
100.0
324
-------
03/31/78
•.—RMA.9
FILE - INK
- CREATED 03/21/78
N.. -AQ_
CATEGORY LABFL
NO. PLANTS USING
RELATIVE ADJUSTED
ABSOLUTE FREQ FRFO
CODE FREQ (PCT) (PCT)
TOTAL
7fl '7-0
-382 S3»0-
460 100.0
VALID CASES
MISSING CASES 38?
CUM
FRFQ
(PCT)
100.0 , 100.0
-MISSING-— 100.0
100.0
.-: RM50... „_„ CHROMIUM GREEN AQ
CATEGORY LABEL
NO. PLANTS USING
VALID CASES
RELATIVE ADJUSTED CUM
ABSOLUTE FREQ FRFQ FREQ •
CODE FREQ (PCT) (PCT) (PCT)
8
TOTAL
.458
460
^.4 100.0 100.0
,p9.6 MISSING. ..-.loo.o.
100.0 100.0
MISSING CASES 458
>
no
1.. :
CATEGORY LABEL
NO. PLANTS USING" ~
I .
| • VALID CASES
ABSOLUTE
COPE FREO
__ ..__ _..__
.— .-•-:.;.. -.-••- 369 .,
TOTAL 460
FREQ
(PCT)
— 80.£
1 0 0 . ff.
'ADJUSTED ".CUM
FREQ FRF.Q
(PCT) (-PCT)
•100.0
MISSING
" 100.0
100.0
91.
MISSING'-CASES 369
325
-------
03/21/78
R.M5H
FILE - INK
- CREATED 03/21/78
SILVER BLUE AO
CATEGORY LABEL
NO. PLANTS USING
ABSOLUTE
CODE FREQ
1
459
460
RELATIVE ADJUSTED
VALID CASES
TOTaL
MISSING CASES 459
FREO
(PCT)
0.2
99.8
ioo.o
FREQ
(PCT)
CUM
FRFQ
(PCT)
100.0 100.0
MISSING loo.O-
100.0
S -RM54_. ._. READ LEAD NOW AO
CATEGORY LAP.EL
NO. PLANTS USING
CODE
F
,~ * "
•OTAL
ABSOLUTE
FREQ
T
4=7
*T-3 /.
460
RELATIVE
FREQ
(PCT)
(
n.7
go .3
7 ~ • -J
ioo.o
ADJUSTED
FREQ
(PCT)
100.0
MISSING
100.0
CUM — _-
FRFQ
(PCT)
100.0
1 n 0 . 0
VALID CASES
MI.SSING CASES 457
-RMS3-
J3L U E -.SI-L^gS—tj
CATEGORY LABEL
\
, -RELATIVE. .ADJUSTED- CUM...
ABSOLUTE FREQ FRFQ FPFQ
CODE FREQ (PCT) (PCT) (PCT)
.VALIO CASES
460 100.0
TOTAl 460, aOO.O
_0 MLSS1NG .CASES— 460..
MISSING
100..0.
100.0
326
-------
- CREATED 03/21/78
I CATEGORY LABEL
j NO. PLANTS USING
-- RELATIVE -ADJUSTED CUM
ABSOLUTE FPEQ FREQ FRFQ
CODE FREQ (PCT) (PCT) (PCT)
TOT«L
0.4 100.0 100.0.
—9-9 . 6. _M ISS ING 100.0-
100.0 100.0
VALID CASES
MISSING CASES 45a
V—RM56....... _ LEAD OR CHROMIUM YELLOW NON AO
CATEGORY LABEL
NO. PLAMTS USING
VALID CASES
90
RELATIVE ADJUSTED CUM
ABSOLUTE FREO FREQ FRFQ
COHE FREn (PCT)
-------
03/21/73
FILE - INK
-'CREATEO 03/21/78
LEAD OR CHROME ORANGE NON AQ
CATEGORY LABEL
NO. PLANTS USING
RELATIVE ADJUSTED CUM
ABSOLUTE FRFQ . FREQ FRFQ
coriE FREQ
J 84 18.3 100.0 100.0
..376 81.7 MISSING ..100.0
TOTAL \ 460 100.0 100.0
VALID CASES
84
HISSING CASES 376
I OMC;Q
MOM.-AQ-
RELATIVE-—AD JUSTE-D -CUM--..
, ABSOLUTE FREQ FREQ FREQ
f CATEGORY LABEL CODE FREQ ^ (PCT)
-------
03/21/7R FILE - INK ' • - CREATED 03/21/78
—-RM61 _.„ COPPER -.OR ..CYANIOE-.-GRFEN NON AQ
CATEGORY LABEL
NO. PLANTS USING
•RELATIVE ADJUSTED- CUM..
ABSOLUTE FRFQ FRFQ FRFQ
CODE FREQ (PCT) (PCT) (PCT)
,M ' '
31.3 100.0 100.0
—-. ,'.^.L.,_::_316 __.. 6fl.z: .MISSING——100.0.---
TOTAL 460 100.0 100.0
VALID CASES
MISSING CASES 316
V-...J?M6'2'.._ ... COPPER OR CYAJMIQE BLUE MON AQ
CATEGORY LAPEL
NO. PLANTS USING
VALID CASES
166
RELATIVE ADJUSTED CUM
ABSOLUTE FREQ FRF.Q " FRFQ
CORE FREO (PCT) (PCT)
TOTdL .
166
294
460
36.1
63.9
lon.o
100.0
MISSING
100.0
100.0
100.0-
CASES 294
> RM63-
i'
VF.P BLJJ£-
CATEGORY LABEL
NO. PLANTS
-HOW—A.O.
VALID CASES
-^.— ,.._. ..:.:_.. RELATIVE ...ADJUSTED—-^. CUM....
ABSOLUTE FREQ FREQ FPEQ
CODE FRFQ (PCT) • (PCT) (P.r.T)
8 • 1 0.2 100.0 100.0
—-.---.- .•:-., . .459 -99.3. MISSING—..'100.0..
100.0 100.0
TOTAL
460
MTSSTNG CASES 459
329
-------
03/21/75?
FILE - INK
- CREATED 01/21/78
RM64
LEAD DRIERS
:
i
/*""""
i
* **
i
•
\
i
aR'SOLUTE
CATEGORY LABEL COnE FREO
NO. PLANTS USING A 140
T?0
TOTAL 460
VALID CASES 140 MISSING CASES 320
RM6S ZTk'f PRj^pc
ABSOLUTE
CATEGORY LABEL , CODE FREO
NO. PLANTS USING ' B '60
4-O.fl
TOT4L 46H
VALID CASES 60 MISSING CASES 40<
RMoo M15U UKlcKa
ABSOLUTE
CATEGORY LA8.EL CODE FREO
NO. PLANTS USING C 37 .
423
TOTAL 460
RELATIVE
FREO
(PCT)
30.4
69.6
100.0
-RELATIVE
FREQ
(PCT)
13.0
R7,P-
100.0
)
. -
RELATIVE
FREO
(PCT)
8.0
92.0
100.0
ADJUSTED
FRF.Q
(PCT)
100.0
MISSING
100.0
/
ADJUS-TED -
FREQ
(PCT)
100.0
MISSING.
iOO.O
••
ADJUSTED.
FREQ
(PCT)
100.0
MISSING
100.0
CUM ....
FRFQ .;.
• (PCT)
100.0
1 0 n * n
' \
i
.. CUM
FRFQ
' (PCT) :
100.0
ion0n
t
CUM.
F"FQ
(RCT)
100.0
100.0
VALID CASES
37
MISSING CASES 423.
330
-------
03/21/73
S.-—RM67L.
F-ILE - INK
XPH.THENAI£_DR.IF.RS-
- CREATED 03/21/78
: RELATIVE . ADJUSTED ' CUM
i . ' • ABSOLUTE FREQ FREQ FREO
I CATEGORY LABEL CODE FREO (PCT) (PCT) (PCT)
|. NO. PLANTS USING o 173 37.6 ~~ 100.0 loo-.o
| .-.: - : - : ... _:__'_2a.7 -6.2.4 MISSING ...loo.o.
j . TOTAL 460 ioo.o loo.o
! ; ; . • _ - _ ._ ; : . ;
i , '' •
'• VALID CASES 173 MISSING CASES 287
V ..RM68 / ZINC SOAPS ; -..---..
i ' '.": ^ - RELATIVE ADJUSTED CUM..
: ABSOLUTE FREQ FREO FREQ
i /CATEGORY LABEL CODE FREQ ' (PCT) (PCT) (PCT)
: NO. PLANTS USING , E 2V 5.2 100.0 10.0.b
...436 .. 94.8 MISSING.... 100.0.
loo.o 10,0.0
VALID CASES 24. MISSIMG "CASES 436 , .
; • .
1 . , . - -
i " ' ' • •
> RM69 LEA.D.. 50 ASS——- '.
-.--.-.. ..—-. • --.-,, RELATIVE-' ADJUSTED. CUM
; • ABSOLUTE FREO FREQ FRFQ
CATEGORY LABEL CpOE FREQ (PCT) (PCT) (PcT)
460 loo.o MISSING 100.0
- -- •.:•"..--TOT.AL - - 460 . 100...0 /._. -100.0
—VALID CASES
,- 0 ,-MISS.lAlG-CASES , 460_.
331
-------
03/21/7R
FILE - INK
- CREATED 03/?l/78
RM70
01 N BUTYL °HTHALATF PLASTTCI7E&S
; CATEGORY LAPEL
• NO. PLANTS USING
VALID CASES
129
RELATIVE ADJUSTED
ABSOLUTE FREQ FREQ
CODE FREQ (PCT) (PCT)
TOTAL
12-9
331
460
28.0
72.0
lon.o
MISSING CASES 331
100.0
HISSING
100.0
CUM
FRFQ
(PCT)
100.0
100.0
>__RM:
: ., - .... .._ RELATIVE— ADJUSTED---.,. CUM...
ABSOLUTE FREQ FREQ FRFQ
! CATEGORY LABEL CODE FREO (PCT) (PCT) (PCT)
NO. PLA.NTS USING , H "7.7.26.." "sTf- lOoV'6 foo".~0~
• .,-.._ _ 434 94_3..-.__.MISSING 100.0. .
| TOT&L 460 100.0 100.0
VALID CASES 26 MISSIMG CASES 434
> -RM72, OIETHYL PHTHALATE PLASTICIZERS ._
: ' ' RELATIVE ADJUSTED CUM
^ CATEGORY LABEL coo'E ^F^^ ^?, "«, ^?,
; NO. PLANTS USlKlG . j . 34 7.4 100.0 100>0
; " '"' — ; 426 92.6 MISSING 100.0
TOTaL 460 100.0 100.0
VALID CASES
34
MISSING CASES
332
-------
FILE.- INK
- CREATED 03/21/7B
,—RM.Z3-
01 2 . FJIHYL.-H&XYL. ..PH.TfcULA.Xg—glaAS
_ ..'. .. •_.'.'.-... .RELATIVE.. . ADJUSTED CUM. -
. ABSOLUTE FREQ FREQ FRFQ
CATEGORY LABEL x .cone. FREO (PCT) (PCT)
NO. PLANTS USING. J 124 27.0 100.0 100.0
. .._-.: >-.., :_- 336 73...0 MIS-SXNG 100.0—_
TOTAL 460 100.0 100.0
'. VALID CASES 124 MISSING CASES 336
•v.. . RM.74.....>. PARAPLEX
. RELATIVE ADJUSTED* CUM...-
. i ABSOLUTE FRF.Q FREO FREQ
i CATEGORY LABEL ' CODE FREO (PCT) (PCT) (PCT)
/• •
< NO. PLANTS USING K 6n r'3.o 100.0 100.0 .
; ,...,.. . .. ._. 4,03 -..87,0 MISSING...—100.0—
I TOTAL 460 100.0 100.0
I . • . -, _ • _
VALID CASES 60 MISSIMG CASES 400
•• - _ _ _ x _.
~ "'" "• " ' '• ' ~" " •"" " ; ' ,-•-. .. —=• -•• -
i
V PM?g Q'.'T^L HFM7YL PHTHftLATE PL/*STTCIZE° '
i . . . .- .
_„- :— . . :. - —RELATIVE .--ADJUSTED-- ' CUM—
ABSOLUTE FREO' FRFQ FRF.Q
| CATEGORY LABEL cone , FREQ (PCTJ CPCT) .. _ 445 96.X MISSING 100.0.-
TOTAL' 460 100.0 100.0
VALID CASES
15
MISSING CASES 445
333
-------
03/21/78
FILE - INK
T- CREATED 03/21/78
RM76
LEAD STABILIZERS
CATEGORY LABEL
t
NO. PLANTS USING
i
VALID CASES
j
S RM7.Z- Z-T-MC— OR.
t
i
i
j,.
,
j CATEGORY LABEL
NO. PLANTS USING
\
I
VALID CASES
i
i
I
s, RM7S. _,„_ .LEAD OR
! CATEGORY LABEL
1
s NO. PLANTS USING
; - -
ABSOLUTE
CODE FREO
M 1
. - - , 459
TOTAL 460
RFLATIVE
FREQ
(PCT)
0.2
99.8
~ loo.o
ADJUSTED
FREQ
(PCT)
100.0
MISSING.
100.0
CUM
FRFQ
(PCT)
100.0
100.0.-
1 MISSING CASES 459
CADMIUM STARTLIZF0*
ABSOLUTE
CODE FREO
N 3
457_
TOTAL 460
PPI ATTVF
FREO
(PCT)
0.7
99. 3
100.0
i
i
J
t
n
t
!
1
.ADJUSTED CUM_ ..!
FREQ FRFQ
(PCT) (PCT) • n
100.0
-MISSLNG
100.0
100.0
inn n
..I
' |.
i
i
J'
3 MISSING CASES 457
PHENOL STABILIZER
ABSOLUTE
CODE FREO
A 23
.437
TOTAL 460
RELATIVE
FREQ
'(PCT)
5.0
95.0
100.0
ADJUSTED
FREQ
(PCT)
100.0
MISSING
100.0
CUM
FRFQ
(PCT)
100.0
100.0
1
; !
--
VALID CASES
23
MISSING,CASES 437
334
-------
03/21/78
FILE - INK
- CPE&TED 03/21/7S
, HH79-
P-HENQ4 WETXIMG AGEM.TS-
CATEGORY LABEL
RELATIVE ADJUSTED CUM
ABSOLUTE FREQ ' FREQ , - FRFQ
CODE FREO (PCT) (PCT) (PCT)
! NO. PLANTS USING : e * 1.7 100.0 100.0
i. :.. , .:_., ' !._ ._.___A52 -98«3 MISSING—. 100..Q ..
| TOTAL 460 100.0 100.0
VALID CASES - R MISSING CASES 452
i '
v RMSQ.--. - MISC WETTING AGENTS -
RELATIVE ADJUSTED " CUM"..
. ABSOLUTE FREQ FREQ FREQ
! CATEGORY LABEL CODE FREO (PCT) -- . , __...,.__.._..._:.,. .-.RELATIVE...ADJUSTED CUM..
i ABSOLUTE FREQ FREQ FREQ
CATEGORY LABEL , ; COHE FREQ (PCT) (PCT) (PCT)
NO. PLANTS USING \ o '? - o".'*.'"' Voo.o" 106.o~~
' —' —• :,.-:.... 45S _.- 99..6 -—MISSING .. 1 00 . 0
TOTAL 461) 100.0 100.0
VALID CASES 2 MISSING CASES
335
-------
03/2i/7ft
03/21/78
RM82
=>HENOL AMTI SKIM AGEMTS
CATEGORY LABEL CODE
'. NO. PLANTS USING E
TOTAL
VALID CASES 65 MISSING
^ DMRT M£DrtipY PRESERVATIVES
j CATEGORY LABEL CODE
NO. PLANTS USING,. F
t
i , , TOTAL
VALID CASES 2 MISSING
RELATIVE
ABSOLUTE FREQ
FREQ (PCT)
6s? 14.1
- 395 8S.9
460 100.0
CASES 395
RFLATTVF
ABSOLUTE FRF.Q
FREO (PCT)
2 0.4
- • • . .
460 100.0
CASES 458
ADJUSTED ClI*
FREO FRFO
(PCT) (PCT)
100.0 100.0 !
MISSING 100.0 n
ioo«o ;
it •
AH fl I
-------
01/21/7S ,
' FILE - INK
- CREATED 03/21/78
P.CP .
CATEGORY LABEL
NO. PLANTS USING
RELATIVE ADJUSTED CUM
ABSOLUTE FREO FREQ FRFQ
FREQ (PCT)' (PCT) (PCT)
H
TOTaL
8
460
1.7 100.0 100,0
_SS.,3.. -MISSING 100.-0.-
100.0 100.0
VALID CASES
MISSING CASES
452
RM86
. .ZINC PRESERVATIVES
CATEGORY LABEL
cone-
.TOTAL
RELATIVE ADJUSTED
ABSOLUTE FREQ FREQ
-FREQ
460
.460
,(PCT>
100.0
100.0
(PCT)
MISSING
100.0
CUM._
FREQ
(PCT)
100.0
VALID CASES
M-ISSIMG CASES . 460...
PMH7
flTHFP
CATEGORY LARFL
—n- -- -.-RELATIVE ADJUSTED CUM-
ABSOLUTE FREQ FREQ FRFQ
CODE FREQ
-------
OU/21/73
FILE - INK
- CREATED 03/21/78
RMQS
MAPHTHA BASED RFSTNS
CATEGORY LABEL
ABSOLUTE
cone FREP
RELATIVE ADJUSTED CUM
FREO FREQ . FRrQ
(PCT) (PCT) (PCT)
NO. PLANTS USING A 36 7.8
424 92.2
• TOTAL 460 100.0
VALID CASES 36 , MISSING CASES 424
i . ' - -
\ OMRQ TnLnFME OP -'^THYLPFM^FME SOLURL
« !
i
t "ELAT-I^F
i ' ABSOLUTE FREQ
I CATEGORY LABEL COnE FREQ (PCT)
i NO. PLANTS USING B 83 18.0-
t 377 a?, n
I TOTAL 460 100. .0
1 VALID CASES 83 MISSING CASES 377
*
|
•
V RM90-. TOLUENE, OR ETHYLBENZENE SOLUBLE RESINS
', RELATIVE
j — • • - ABSOLUTE FREO
i CATEGORY LABEL COriE FREO (PCT)
i NO, PLANTS USING c 62 13.5,
398 86.5
1 TOTAL 460 100.0
i
i
100.0 100.0 i
MISSING 100.0 -,
100.0 '
i
/ . i
i
ADJUSTED--. CUM :
FRFQ FRFQ
(PCT) (PCT) j
100.0 100.0
MISSING 100.0
100.0
ADJUSTED CUM .
FREQ FRfQ
(PCT) (PCT)
100.0 100.0
' MISSING 100.0 -.-
100.0'
VALID CASES
62
MISSING CASES 398
338
-------
03/21/7R
FILF - INK-
- CREATED 03/31/78
CATEGORY LABEL
NO. PLANTS USING
CODE
„ RELATIVE - ADJUSTED CUM
ABSOLUTE FPEQ FREQ FRFQ
FREO (PCT) (PCT)
-------
03/21/7H
FILE - INK
- CREATF.O 03/?l/78
RM94
TOLUFME OR -MAPHTHA SOLUBLE POLYESTER
CATEGORY LAPEL
NO. PLANTS USING
VALID CASES
41
RELATIVE ADJUSTED CUM
ABSOLUTE FREQ FREQ " FRFQ
COOE FREO (PCT) (PCT) (PCT)
TOTAL
41 8.9
419 91.1
«• *«•««••* ••••«,•••••
. 460 100.0
CASES 419
100.0 100.0
MISSING ,. 100.0
100.0
_- RELATIVE--ADJUSTED.-. CUM.—
•ABSOLUTE FREQ F.RFQ FRFQ
COOE FREO (PCT) (PCT) (PCT)
CATEGORY 'LABEL
NO. PLANTV'usiNG' ""'"""^"""""""H^ ~39 "~~.B.5 100.0 100.0.
_ ;_ 42]' .. _^ 91.5 MISSING. 100.0
TOTAL 460 100.0 100.0
VALID CASES 39 MISSIMG CASES 421
, RM96 . TOLUENE SOLUBLE.POLYAMIDE RESTNS —-•
RFLATIVE ADJUSTED CUM
ARSCLUTE FREO FREQ F^FQ
CATEGORY LABEL CODE FREO (PCT
NO. PLANTS USING i 49 10.7 100.0 100.0
411 89.3 ' MISSINT, 100,0
TOTAL 460 100.0 100.0
VALID CASES
49
MISSING CASES 411
340
-------
03/21/7K
FILE - INK
- CREATED 03/21/78
J3W.97 .. T-OLUENE.-SnLUSL-E-UREA-RES.I-HS—
CATEGORY LAREL
NO. PLANTS USING'
VALID CASES
. ---RELATIVE ADJUSTED CUM.
ABSOLUTE FREQ FREQ FREQ
COriE FREO (PCT) (PCT) (PCT)
TOTAL
29 6.3
_4ai. ; -S3 .7
461 100.0
100.0 100.0
MISSING- 100.0.--.
100.0
29
MISSIMG CASES 431
S -RM98 ....... NAPHTHA SOLUBLE
MELAMINE RESINS
CATEGORY LABEL
NO. PLANTS USING
RELATIVE ADJUSTED CUM
ABSOLUTE FREO FREQ FREO
CODE FREO (PCT) (PCT)
.-.-,- .....417
TOTAL 460
9.3
90.7
100.0
100.0
MISSING
100.0
100.0
100..CL
VALID CASES
43
MISSING CASES 417
I,
..VTM.Y1—rm
CATEGORY LABEL
NO. PLANTS USING
-:_.... .,._.....__,. ,__ .-RELATIVE - ADJUSTED- . CUM...
ABSOLUTE FREQ FREQ FRFQ
COOE FREQ (PCT) (PCT) (PCT)
TOTAL
91
,369.
• *» *»••<•
460
19.8 100.0 100.0
...80.2 -..MISSING .. 100.0
100.0 100.0
VALID CASES
91
CASES 169
341
-------
03/21/7P FILE - TN* - CREATED 03/21/78
RM100 VIMYL CHLORIDE DERIVED
CATEGORY LABEL
NO. PLANTS USING
VALID CASES
11
RELATIVE ADJUSTED
ABSOLUTE FREQ FREQ
CODE
A
TOTAL
CUM
FREQ
(PCT3
FREO (PCT) (PCT)
if 2.4 100..0 _ 100.0
449 .. 97.6 - MISSING_.. -100.0-
460 100.0 ,100.,0
MISSING CASES 449
OP
CATEGORY LABEL
SnL'-'ql-E PV ALCOHOL
RELATIVE— ADJUSTED CUM_
ABSOLUTE FREQ FREQ FREO
COOE FREQ (PCT) (PCT) (PCT)
NO. PLANTS USING
B 2?
43S.
TOTAL" 460
4.R 100.0 100.0
_9.5 . 2 MISSI-NG 10 0 . 0_
100.0 100.0
VALID CASES
22
MISSING CASES 438
l,_RM102_ _- VINYL CHLORIDE VlNYLIDENE CHLORIDE
CATEGORY LABEL
NO. PLANTS USING
VALID CASES
TOTAL
9
451
460
MISSIMG CASES
RELATIVE ADJUSTED CUM
ABSOLUTE FPEQ FREQ
COliE 'FREO (PCT) (PCT)
2.0 1,00.0 100.0
98.0 MISSING 100.0,
100.0 100.0
342
-------
03/21/79
FILE - INK
- CREATED 0.1/21/78
.RM 1 03.
CATEGORY LAPEL
NO. PLANTS USING
— . RELATIVE ADJUSTED
ABSOLUTE FREQ FREQ
CODE FREQ (PCT) (PCT)
o
TOT4L
90 19.6
37.n _. _80..4....
460 100.0
100.0
-MISSING-
100.0
CUM .
FRFQ
(PCT)
100.0
100.0 -
VALID CASES
90
MISSING CASES 370
RR104 ..-..TOLUENE 'SOLUBLE
-ACRYLIC SOLUTIONS
LABFU .
NO. PLANTS USING
conE
E
TOTAL
-V' -
FREQ
78
—382
460
RELATIVE ADJUSTED
FREQ
(PCT)
17.0
83.0
^^ •»*•«• *
100.0
100.0
MISSING
100.0
VALID CASES
78
MISSING CASES 382
CUM
FR'FQ
(PCT)
100.0
100.0
>—BM4-OS T.niJtFME SOLUS|=g-au8agj?.S-
WTEBOW UIBEU
NO. PLANTS USING ."
COHE
F
TOTAL
- .--.RELATIVE ADJUSTED
FREQ
(PCT)
.381 .....
460
-—82.8
100.0
VALID CASES
79
CASES 38*1
100.0
MISSING
100.0
• CUM_-
FRFQ
(PCT)
100.0
100.0
343
-------
03/21/78
FILE: -
- CREATED 03/P1/78
RM106
PHENOLIC RESIMS
CATEGORY LABEL
RELATIVE ADJUSTED CUM
ABSOLUTE FREO FREQ F«FQ
CODE FREO (-PC TV (PCT) (PCT)
NO. PLANTS USING
VALID CASES 157
.5
t
• CATEGORY LABEL
NO. PLANTS USING
t
t
VALID CASES 53
(
V _RM105 ETHYLBENZENE
j CATEGORY LABEL
NO. PLANTS USING
G 157 34.1
303 65.9
TOTAL 460 100.0
MISSING CASES 303
RFLAT.IVf-
ABSOLUTE FPEQ
CODE FREO (PCT)
H 53 11.5
TOTAL 460 100.0
MISSING CASES 407
OR . . _ , PHENOL SOLUBLE OLc.
RELATIVE
ABSOLUTE FREO
COOE FREO (PCT)
'I 96 .20.9
..364 79.1
TOTAL 460 100.0
100.0 100.0
MISSING 100.0 -
100.0
.ADJUSTED CUM
FREQ FREQ
(PCT) (PCT)'
100.0 100.0
-MISSING lQit<>
100.0
ADJUSTED CUM
FREQ FRFQ
(PCT) (PCT)
100.0 100.0
MISSING 100.0 -
100,0
• -
'r '.
- ' T
1
"1
' !
|
J
'
VALID CASES
96
MISSING CASES 364
344
-------
01/21/73
FILE - TN*
- CREATED 03/21/78
]. ,_J?M109
! CATEGORY LABEL
; NO. PLANTS USING
i
• - RELATIVE ADJUSTED CUM
ABSOLUTE FREQ FRFQ FREQ
CODE FREQ (PCT) (PCT) (PCT)
TOTAL
7<5
-3as.
460
16.3 lOOoO 100.0
-.33. 7 ..-.-MISSING 100.0-
lon.o 100.0
VALID CASES
75
CASES 385
S - RM11Q . TOLUENE SOLUBLE-MALETC SOLUTIONS
-;— CATEGORY LABEL
NO. PLANTS USING
VALID CASES
44-
COnF
K
TOTAL
- • RELATIVE ADJUSTED
ABSOLUTE FREQ FRFQ
FREO
.--4L6
460
(PCT)
CUM .
FREQ
(PCT)
(PCT)
9.6 100.0 100.0
90.4 . . MISSING -....1.00,0..
100.0 100.0
MISSING CASES 416
>—BM4-U,
TDl IIFMF
RE5TMS-
CATEGORY LABEL
NO. PLANTS usIMG
^..!-:_._:.,_,_:•__-_ ...RELATIVE...-ADJUSTED. CUM,..
. ABSOLUTE FREQ FREQ FREQ
CODE FREQ (PCT) -(PCT)
-------
03/21/7*
FILE - IN*
- CREATED 03/21/78
RM11? MISC PtblNb
RELATIVE
ABSOLUTE FPEQ
CATEGORY LABEL CODE FREO (PCT)
NO. PLANTS USING M 62 13.5
398 86.5
TOTAL 460 100.0
VALID CASES 6? MISSING CASES 398
V, HMl.l-J MbMltlMt
RP1 ATTVF .
ABSOLUTE FREQ
CATEGOR-Y—frffBEl. CODE FREQ (PCT)
NO. PLANTS USING . ... A 6 1.3
454 9fi 7
' TOTAL 460 100.0
VALID CASES 6 MISSING CASES 454
V. RMilA BENZENE TOLUENE MIXTURES
: . RELATIVE
ABSOLUTE FREO
'; CATEGORY LABEL COnE FREO _ (PCT)
NO. PLANTS USING s 3 0.7
457 ' 99.3
TOTAL 460 100.0
VALID CASES 3 MISSING CASES 457
ADJUSTED CUM
FREO FREO
(PCT) (PCT)
100..0 100.0 i
MISSING 100.0
1 100.0
« s-
3
1
-ADJUSTED ..-CUM 1
FREQ FRP-Q
(PCT) (PCT)
100.0 100.0
! , •' - '. 1
MISSING- 100. a
100.0
ADJUSTED CUM ...
FREO FRc-Q
(PCT) (PCT)
100.0 100.0
MISSING 100.0
too.o
346
-------
03'/21/7R
FILE - INK
- CREATED 03/21/78
V—BM-ILS,—
CATEGORY LABEL CODE
NO. PLANTS USING c
TOTaL
.
VALID CASES - 160 MI^SlMG
ABSOLUTE
FREO
16(1
30 n
460
CASES " 300
y
^ - RM116 ..,.. TOLUENE ETHYLBENZFNE MIXTURES
-
• ABSOLUTE
CATEGORY LABEL CODE 'FREO
NO. PLANTS USING D
L •
TOTAL
4
456
460
FPEQ
(PCT>
34.8
6^.2
100.0
RELATIVE
FPEQ
tPCT)
0'.9
99.1
100..0
FRFQ
(PCT)
100.0
MISST-NG,.-
100.0
ADJUSTED
FREO
(PCT)
,100.0
MISSING
100.0
FRFQ
(PCT)
100.0 ,
100.0
CUM
FRFQ
(PCT)
100.0
1,00.0'. .
VALID CASES
MISSING CASES
\
456
THY
CATEGORY LABEL |
NO. SLANTS USING
. , '. RELATIVE- ADJUSTED CUM..
ABSOLUTE FREQ ; FREQ , FREQ-
COOE FREO (PCT) (PCT)
TOTAL
29 6.3 100.0
.431- — . 93.7 ..... MISSING
460 100.0 100.0
100.0
100,.0
VALID CASES
29
MISSING CASES ' 431
347
-------
03/21/7*
FILE - IN*
- CREATFO 03/21/7(3
RM11S
ISOPHORONE
ABSOLUTE
CATEGORY LABEL COOE FREQ
NO. PLANTS USING . F 30
.. , .430
TOTAL 46n
VALID CASES 30 MISSING CASES 430
ABSOLUTE
CATEGORY LABEL CODE FREQ
NO. PLANTS USING G i
•
TOTAL 460
.VALID CASES 1 MISSING CASES 4=59
•.—RM12.0 JCHLOROBENZENE .*
CATEGORY LAPEL COOE ^F^EQ^
460
TOTAL 460
RELATIVE
FRFQ
(PCT)
6.5
93. 5
100.0
..._..
RELATIVE-
FREQ
(P.CT)
0.2
39.8
100.0
.
RELATIVE
FPFQ
(PCT)
100.0
100.0
ADJUSTED
FREQ
(PCT)
100.0
MISSING
100.0
- - -
- . AD JUSTFOT
FREQ
(PCT)
1 00 . 0_.
MISSING-
100.0
ADJUSTED
FREQ
(PCT)
MISSING
100.0
CUM
FRFQ
(PCT)
100.0
100..0 -,
J
—
.." I
FREQ
(PCT)
100.0
-.10.0.. 0
, i
; - '•
CUM
FRFQ
(PCT)
100,0
VALID CASES
MISSING CASES
348
-------
03/21/78 ,
>—am 21—
FILE - INK
- CREATED 03/21/78
CATEGORY LABEL
RELATIVE ADJUSTED
- AHSOLUTE FREO FREQ-
COOE FREO (PCT) (PCT)
CUM
FRFQ
-•-.-.. : 4fio ion.o MISSING 100.0
----- - ----- ,- . -.,.. TOTAL . ..-46Q ____ 100.0 ..... ........ 100. Q....
..—VALID CASES _____ , ... .0_ ..... . MISSING -.CASES ______ 4.6fl _ _ ....... _______________ ; .....
y. -RM122-- - 1-2-OICHLOROETHANF. , , ___
' RELATIVE ADJUSTED CUM
: ' „ - -" . ' ABSOLUTE FREO FRF.Q FRFQ
CATEGORY LABFL COOE FREO (PCT) (PCT) (PCT)
: . '"" ^60 100.0 MISSING 100.0
< • ,• '---•-<. .TOTAL 460 100.0 100.0 .. ......
: v V41 Tn na«?F«; o
i '
1 . -
I , •
i - . ....
L PMi?3 _ 1 1 It 1
1 ________ ....... ________ . ...._...,,.,: _______ ... ,,-.,: ..... — RELATIVE. ADJUSTED CUM
\ '.-•-•• ABSOLUTE FREQ FREO FRFO
CATEGORY LABEL CODE FREO (PCT) (PCT) (PCT)
NO. PLANTS USING' K 41 8.9 100.0 100.0
________ .. ... ; ......... _ ,.41.9.. .:...-. 91.1... MISSING 100.0
• TOTAL 460 " 100.0 .100.0
VALID CASES
41
MISSING CASES
419
349
-------
03/21/78
FILE - IN*
- CREATED 03/P1/7S
RM124
I«lt2 TRICHLOROFTMANF
CATEGORY LABEL
NO'. PLANTS USING
COHE
TOTAL
BSOLUTE
FREO
1
. ..459
460
RFLATIVE
(PCT)
0.2
99. S
100.0 '
ADJUSTED
FREQ
(PCT)
100.0
MISSING
100.0
CUM
FRFQ
(PCT)
100.0
100.0.
VALID CASES
MISSING CASES 459
' CATEGORY LABEL
RELATIVE—ADJUSTED— -CUM-
; ABSOLUTE FRFQ FRFQ FRFQ
CODE FREO (PCT) (PCT) (PCT)
460
-VALID CASES ,.0 M1SS.1MG _CAS£S 46H_
loo.o MISSING 100.0
.1.0 0 .. 0 lU 0 ..0
350
-------
FILE -
- CREATED 03/21/78
.-RM126
CHLOROFORM
! CATEGORY LABEL
f
; NO. PLANTS USING
VALID CASES
cone
TOTflL
MISSING CASES 459
RSOLUTE
PREO
1
459
460
RELATIVE
FREQ
(PCT)
0.2
99.3
100.0
ADJUSTED
FREQ
-------
03/21/73
FILE - IN*
- CREATED 03/21/78
. RM.12<3
CATEGORY LABEL
t NO'. PLANTS USING
-.-•RELATIVE ADJUSTED CUM
ABSOLUTE FREO FREQ FRFQ
CODE FREO (PCT) (PCT) (PcTJ
, A 13 2.8 100.0 100.0
442 . 9.7.2— MISSING.- . 100,0.
TOTAL 460 100.0 100.0
VALID CASES
13
MISSING CASES 447
..RM130 THICHLOROETHYLENE
CATEGORY LABEL
NO. PLANTS USING
CODE
8 ,
•OTAL
ABSOLUTE
FREO
3?
42B
460
RELATIVE
FREO
((PCT)
7.0
93.0
100.0
ADJUSTED
FREQ
(PCT)
100.0
MISSING .
100.0
CUM
FRP-Q
(PCT)
100.0
100.0
VALID CASES
32
MISSING CASES
ETHYLEME DICMLOpTnE
CATEGORY LAPEL
RELATIVE ADJUSTED. • CUM.
ABSOLUTE FREQ FREQ FRrQ
CODE FREO (PCT) (PCT) (PCT)
—.VALID.,CASES .
100.0 MISSING 100.0
.T.D.TAL- 460 100.0. 100.0 .._
.0 HISSING-CASES 460 _. . .1
352
-------
RM132
FILE -
PFRCHLOROETHYLEME
- CRFATED 03/21/78
RELATIVE ADJUSTED CUM
t ABSOLUTE FRFQ FREQ FRFQ
• CATEGORY LABEL COHE FREQ CPCT> 8-M.1.33———MAP-HTA : — : : :
| .... ;..,. .......' RELATIVE ADJUST-EC CUM
; . . ABSOLUTE FREQ FREQ FRF.P
j CATEGORY LABFL COOE • FREQ (PCT)
-------
-------
-------
Special
Fourth-Class
Rate
Book
United States
Environmental Protection
Agency
Washington DC 20460
Official Business
Penalty for Private Use 5300
-------