-:United "States ;'y:> "y^--
Environmental Protection".
Office of Water
                Office i of^VaterReguiatjbnf;,
                : Irjdu itrial Technology piyigi
                '-Was iingttJfC DC 20460 " \f ;
Nonferrous  Metals
Manufacturing      I
Pciirtt Sste*r*,!.?

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                  ORGANIZATION OF THIS DOCUMENT
This development document for the nonferrous metals manufacturing
category  consists  of  a  general  development  document   which
considers  the general and overall aspects of the regulation  and
31  subcategory specific supplements. These parts  are  organized
into 10 volumes as listed below.

The information in the general document and in the supplements is
organized  by sections with the same type of information reported
in  the same section of each part.  Hence to find information  on
any  specific aspect of- the category one would need only look  in
the  same  section  of  the general  document  and  the  specific
supplements of interest.

The ten volumes contain contain the following subjects:
   Volume I

   Volume II



   Volume III




   Volume IV




   Volume V




   Volume VI




   Volume VII
General Development Document

Bauxite Refining
Primary Aluminum Smelting
Secondary Aluminum Smelting

Primary Copper Smelting
Primary Electrolytic Copper Refining
Secondary Copper Refining
Metallurgical Acid Plants

Primary Zinc
Primary Lead
Secondary Lead
Primary Antimony

Primary Precious Metals and Mercury
Secondary Precious Metals
Secondary Silver
Secondary Mercury

Primary Tungsten
Secondary Tungsten and Cobalt
Primary Molybdenum and Rhenium
Secondary Molybdenum and Vanadium

Primary Beryllium
Primary Nickel and Cobalt
Secondary Nickel
Secondary Tin
   Volume VIII Primary Columbium and Tantalum
               Secondary Tantalum
               Secondary Uranium

   Volume IX   Primary and Secondary Titanium
               Primary Zirconium and Hafnium

   Volume X    Primary and Secondary Germanium and Gallium
               Primary Rare Earth Metals
               Secondary Indium

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                DEVELOPMENT DOCUMENT

                         for

    EFFLUENT LIMITATIONS GUIDELINES AND STANDARDS

                       for the

NONFERROUS METALS MANUFACTURING POINT SOURCE  CATEGORY

                      VOLUME II

                  Bauxite Refining
              Primary Aluminum Smelting
             Secondary Aluminum Smelting

                  William K. Reilly
                    Administrator
                Rebecca Hanmer,f  Acting
          Assistant Administrator  for Water
              Martha Prothro,  Director
      Office of Water Regulations  and Standards
                            \
                       mj
            Thomas P.  O'Farrell,  Director
           Industrial  Technology  Division
             Ernst P.  Hall,  P.E.,  Chief
               Metals  Industry Branch
                         and
              Technical  Project Officer
                     May 1989
        U.S.  Environmental  Protection Agency
                   Office of  Water
      Office  of Water  Regulations and Standards
           Industrial  Technology Division
              Washington, D.  c'.  20460

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11

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                        TABLE OF CONTENTS
Supplement
Paqe
Bauxite Refining
     505
Primary Aluminum Smelting
     591
Secondary Aluminum Smelting
     859
For detailed contents see detailed contents list in
individual supplement.
                               111

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IV

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NONFERROUS METALS MANUFACTURING POINT SOURCE CATEGORY
           DEVELOPMENT DOCUMENT SUPPLEMENT
                       for the
            Bauxite Refining Subcategory
                  William K. Reilly
                    Administrator
                   Rebecca Hanmer
      Acting Assistant Administrator for Water
              Martha Prothro, Director
      Office of Water Regulations and Standards
            Thomas P.  O'Farrell, Director
           Industrial  Technology Division
             Ernst P.  Hall,  P.E.,  Chief
               Metals  Industry Branch
                         and
              Technical Project Officer
                     May 1989
        U.S.  Environmental Protection Agency
                   Office of Water
      Office  of Water Regulations and Standards
           Industrial Technology Division
              Washington, D. C.   20460
                         505

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506

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                 BAUXITE REFINING SUBCATEGORY
                        TABLE OF CONTENTS
Section
                                             Page
I

II

III
IV
V
SUMMARY AND CONCLUSIONS

RECOMMENDATIONS

INDUSTRY PROFILE

Description of Bauxite Refining Processes
Raw Materials
Bauxite Grinding and Digestion
Red Mud Removal and Liquor Purification
Precipitation and Classification
Calcination
Process Wastewater Sources
Other Wastewater Sources
Age, Production, and Process
Profile

SUBCATEGORIZATION

Factors Considered in
Subcategorization
Factors Considered in Subdividing
The Bauxite Refining Subcategory
Other Factors
Type of Plant
Raw Materials
Plant Location

WATER USE AND WASTEWATER
  CHARACTERISTICS

Wastewater Characteristics Data
Data Collection Portfolios
Field Sampling Data
Wastewater Characteristics and
Flows by Building Block
Digester Condensate
Barometric Condenser Effluent
Carbonation Plant Effluent
Mud Impoundment Effluent
513

517

519

519
520
520
521
522
523
524
524
524


531

531

531

532
532
532
533

535
                                                            536
                                                            536
                                                            536
                                                            538

                                                            538
                                                            538
                                                            538
                                                            539
                               507

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 Section
                  BAUXITE REFINING  SUBCATEGORY
                   TABLE  OF CONTENTS  (Continued)
VI
VII
VIII
 SELECTION  OF  POLLUTANT  PARAMETERS                  555

 Conventional  and Nonconventional Pollutant         555
  Parameters
 Conventional  and Nonconventional Pollutant         555
  Parameters  Selected
 Toxic Priority Pollutants                          556
 Toxic Pollutants Never  Detected                    556
 Toxic Pollutants Never  Found Above Their           558
  Analytical  Quantification Level
 Toxic Pollutants Present Below Concentrations      559
  Achievable  by Treatment
 Toxic Pollutants Detected in a Small Number of     559
  Sources
 Toxic Pollutants Selected for Further              559
  Consideration for Limitation

 CONTROL AND TREATMENT TECHNOLOGIES                 569

 Current Control and Treatment Practices            569
 Mud Impoundment Effluent                           569
 Control and Treatment Options                      570
 Option E                                           570

 COSTS OF WASTEWATER TREATMENT AND CONTROL          571

 Treatment Options Costs for Existing Sources       571
 Option E                                           571
 Cost Methodology                                   571
 Nonwater Quality Aspects                           572
 Energy Requirements                                572
 Solid Waste                                        572
Air Pollution                                      572
IX
BEST PRACTICABLE TECHNOLOGY CURRENTLY AVAILABLE   575
                               508

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                 BAUXITE REFINING SUBCATEGORY
                  TABLE OF CONTENTS (Continued)
Section
                                             Page
X
XI
XII

XIII
BEST AVAILABLE TECHNOLOGY                         577
ECONOMICALLY ACHIEVABLE

Technical Approach to BAT                         577
Option E                                          577
Industry Cost and Pollutant. Removal Estimates     579
Pollutant Removal Estimates                       579
Compliance Costs                                  579
BAT Option Selection                              579
Regulated Pollutant Parameters                    580
Effluent Limitations                              581
Recommended Guidance for BAT                      581
Effluent Limitations for the Bauxite Refining     581
  Subcategory

NEW SOURCE PERFORMANCE STANDARDS                  585

Technical Approach to NSPS                        585
Option E                                          585
NSPS Option Selection                             586
Regulated Pollutant Parameters                    586
New Source Performance Standards                  586
Recommended Guidance for NSPS for                 586
the Bauxite Refining Subcategory

PRETREATMENT STANDARDS                            587

BEST CONVENTIONAL POLLUTANT CONTROL TECHNOLOGY    589
                               509

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                  BAfJXITE REFINING SUBCATEGORY
 Tables


 III-l




 III-2


 III-3



 V-l



 V-2



 V-3




 V-4





V-5



VI-1
                          LIST OF TABLES
        Title
 Initial Operating Year (Range)
   Summary of Plants in the
   Bauxite Refining Subcategory
   by Discharge Type

 Production Ranges for the Bauxite
   Refining Subcategory

 Summary of Bauxite Refining
   Subcategory Processes and
   Associated Waste Streams

 Water Use and Discharge Rates for
   Mud Impoundment Effluent
   (liters/yr)

 Bauxite Refining  Subcategory
   Digester Condensate Sampling
   Data

 Bauxite Refining  Subcategory
   Barometric  Condenser  (Hot
   Well)  Discharge Raw
   Wastewater  Sampling Data

 Bauxite Refining  Subcategory
   Carbonation Plant Effluent
   Raw Wastewater  Sampling
   Data

Bauxite Refining  Subcategory
  Mud Lake Discharge  Raw
  Wastewater Sampling Data

Frequency of Occurrence of
  Priority Pollutants Bauxite
  Refining Raw Wastewater
 528


 526



 540



 541



 544




 547





549



561
                               510

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                 BAUXITE REFINING SUBCATEGORY
                   LIST OP TABLES (Continued)
Tables

VI-2

VI-3


VIII-1




X-l


X-2
       Title

Toxic Pollutants Never Detected

Toxic Pollutants Never Found
  Above Their Quantification Level

Cost of Compliance for the
  Bauxite Refining Subcategory
  Direct Dischargers

Pollutant Removal Estimates
  Bauxite Refining Subcategory

Cost of Compliance for the
  Bauxite Refining Subcategory
568

567


573




582


583
                               511

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                 BAUXITE REFINING SUBCATEGORY
                         LIST OF FIGURES
Figures
       Title
Page
III-l

III-2



V-l


V-2


X-l
Bauxite Refining Process

Geographic Locations of the
  Bauxite Refining Subcategory
  Plants

Sampling Sites at Bauxite
  Refining Plant A

Sampling Sites at Bauxite
  Refining Plant B

Option E Treatment Scheme for
  the Bauxite Refining
  Subcategory
527

529



552


553


584
                               512

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              BAUXITE REFINING SUBCATEGORY  SECT - I
                            SECTION I

                     SUMMARY AND CONCLUSIONS
On April 8,  1974,  EPA promulgated effluent limitations based on
best  practicable  technology  currently  available  (BPT)    and
best   available   technology  economically   achievable   (BAT),
standards of performance for new sources (NSPS) and  pretreatment
standards   for  new  sources  (PSNS).   In   each    case,   the
limitations  and  standards  required  no  discharge  of  process
wastewater   pollutants with  an  allowance  for   discharge   of
monthly  net precipitation (i.e., the difference in water  volume
between   precipitation   and  evaporation   in   a   one   month
period)   that  accumulates in the impoundments used  by  bauxite
refineries  to  store  the  undigested solids  produced   in  the
refining  process.  This document and the  administrative  record
provides  the  technical basis for  review   of  the  promulgated
effluent limitations and standards.

The  bauxite  refining  subcategory consists of 8 plants.  Of the
8  plants, three discharge directly to rivers, lakes, or  streams
and five achieve zero discharge of process wastewater.

EPA first studied the bauxite refining subcategory  to  determine
whether   differences   in   raw   materials,   final   products,
manufacturing processes, equipment, age and size  of  plants,  or
water  usage,  required  the  development  of  separate  effluent
limitations  and  standards  for  different   segments   of   the
subcategory.   This  involved  a  detailed analysis of wastewater
discharge and treated effluent characteristics, including (1) the
sources and volume of water used, the  processes  used,  and  the
sources  of  pollutants and wastewaters in the plant; and (2) the
constituents of wastewaters,  including priority pollutants.    As
a  result,    four    subdivisions   have  been  identified   for
this  subcategory that warrant separate   effluent   limitations.
These include:

 o Digester Condensate
 o Barometric Condenser Effluent
 o Carbonation Plant Effluent
 o Mud Impoundment Effluent

EPA  also  identified  several  distinct  control  and  treatment
technologies (both in-plant and end-of-pipe)  applicable  to  the
bauxite   refining   subcategory.    The   Agency  analyzed  both
historical and newly generated data on the performance  of  these
technologies,   including  the  non-water  quality  environmental
impacts    and    air    quality,     solid    waste  generation,
and   energy requirements.     EPA  also  studied  flow  reduction
                               513

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reported
visits.
              BAUXITE REFINING SUBCATEGORY  SECT - I
in  the  data collection portfolios  (dcp)    and  plant
Engineering costs were prepared for each discharging  plant  (and
one  zero  discharger)  for  the  control  and  treatment  option
considered for the subcategory.  These costs were  then  used  by
the  Agency  to estimate the impact of implementing the option in
the subcategory.  For this  control  and  treatment  option,  the
number  of  potential closures, number of employees affected, and
impact on price were estimated.  These results are reported in  a
separate  document  entitled  "The  Economic  Impact  Analysis of
Proposed Effluent Limitations Guidelines and  Standards  for  the
Nonferrous Smelting and Refining Industry."

After examining the various treatment technologies being operated
in   the  subcategory,  the  Agency  has  identified  BPT  to  be
equivalent to the existing promulgated BPT  effluent  limitations
published  on  April  8,  1974 (40 CFR Part 421 Subpart A).  This
requires  no  discharge  of  process  wastewater  pollutants   to
navigable   waters,   while   permitting  the  discharge  of  net
precipitation from red mud lake impoundments.   Minor  amendments
to  the    regulatory   language  are  promulgated    to  clarify
references    to    fundamentally    different     factors  (FDF)
considerations    under      40     CFR    Part      125      and
references  to pretreatment standards under 40 CFR Part 128.   As
a  result,   the bauxite  refining  subcategory  will  not  incur
any  incremental  capital or annual costs to comply with the  BPT
limitations.

For BAT,  the Agency considered revising the  promulgated  BAT to
include   treatment   of   the  allowable  discharge    of    net
precipitation   from  mud  impoundments  by  pH  adjustment   and
activated  carbon  adsorption technology for removal  of  organic
pollutants.    This   potential   revision  was  based   on   new
data  collected by the Agency  since  the  previous  promulgation
that  indicated    the   presence  of   phenolic   compounds   at
treatable   concentrations  in  the  mud  impoundment   effluent.
Since   proposal   the  Agency  has   received   newly  collected
data  for  the red mud lakes showing levels below  the  limit  of
detection for all phenolic compounds except  phenol. As a result,
the  Agency  has  decided not to  establish  additional  national
effluent   limitations   guidelines  and  standards   for    this
subcategory  but  rather  to  recommend  guidance  to  permitting
authorities  to  deal  with  any  site-specific  high  levels  of
phenolics.

The technical  basis  of  NSPS  is  equivalent  to  the  existing
promulgated  BAT.   In  selecting  NSPS,  EPA recognizes that new
plants have the  opportunity  to  implement  the  best  and  most
efficient   manufacturing  processes  and  treatment  technology.
However,  no  such  processes  or   treatment   technology   were
considered  to meet the NSPS criteria.  Therefore, the technology
basis of  BAT  has  been  determined  as  the  best  demonstrated
technology,  the  technology basis of NSPS.   The Agency was also
considering   the  application  of pH  adjustment  and  activated
                               514

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              BAUXITE REFINING SUBCATEGORY  SECT - I


carbon adsorption technology to the mud impoundment effluent  for
new  sources.     The  Agency  is not revising   the  promulgated
NSPS,  but is recommending guidance to permitting authorities  to
deal  with  any  site-specific  high  levels  of phenolics.

The  limitations  and  standards for 13PT, BAT, NSPS, and PSNS are
presented in Section II.
                               515

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BAUXITE REFINING SUBCATEGORY  SECT - I
 THIS PAGE INTENTIONALLY LEFT BLANK
                 516

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             BAUXITE REPINING SUBCATEGORY  SECT-II




                         SECTION II

                      RECOMMENDATIONS
EPA   is   not changing the existing promulgated BPT   for    the
bauxite  refining  subcategory.   The  regulation  establishes no
discharge of process wastewater pollutants with an allowance  for
discharge  of  net  precipitation  from the mud impoundment.  The
technology basis for BPT  is  impoundment  and  recycle  for  all
process wastewater.

EPA  is  not substantially modifying the existing promulgated BAT
limitations. However, the Agency is providing guidance in Section
X for the control of phenolics.

Similar   to  BAT,  EPA  is  not  substantially   modifying   the
existing   promulgated   NSPS,  but is recommending  guidance  in
section XI for the control of phenolics.

EPA   is   not promulgating PSES limitations  for   the   bauxite
refining  subcategory  because  there are  no  existing  indirect
dischargers.

EPA is not modifying the existing promulgated  PSNS  since  it is
unlikely  that  any  new  bauxite sources could be constructed as
indirect dischargers.

EPA  is  not  promulgating best  conventional  pollutant  control
technology (BCT) limitations at this time.
                               517

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BAUXITE REFINING SUBCATEGORY  SECT-II
  THIS PAGE INTENTIONALLY LEFT BLANK
                  518

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             BAUXITE  REPINING  SUBCATEGORY   SECT-III





                            SECTION  III

                         INDUSTRY PROFILE
 This  section of  the bauxite  refining supplement describes  the  raw
 materials  and   processes  used  in  refining  bauxite  to  produce
 alumina and presents a profile of the alumina  plants   identified
 in  this  study.  For a discussion of the purpose, authority,  and
 methodology for  this study and a general description of  the  non-
 ferrous  metals  manufacturing  category, refer to Section III of
 the General Development Document.

 EPA promulgated  effluent limitations for BPT and BAT, new  source
 performance standards, and pretreatment standards for new  sources
 for   the bauxite refining subcategory on April 8, 1974 as  Subpart
 A  of  40  CFR   Part  421.   The  pollutants  considered   in   the
 development  of  those regulations included alkalinity, pH; total
 dissolved solids, total suspended solids, and sulfate.
The Clean Water Act of 1977 mandates the achievement of  effluent
limitations    requiring    the    application    of   BAT    for
toxic  pollutants.    In  keeping  with this emphasis  on
pollutants,   EPA    is  re-examining  the  discharge
pollutants  from  process  wastewater   impoundments
bauxite   refining subcategory.
     toxic
of   toxic
 in    the
Most  of  the alumina produced by bauxite refiners is sold to the
primary aluminum industry.  Aluminum metal  is  widely  used  for
building  and  construction  materials, transportation equipment,
and containers and packaging  products.   The  remainder  of  the
alumina   is   sold  to  the  chemical,  abrasive,  ceramic,  and
refractory industries for the manufacture  of  products  such  as
chemical   alums,   activated   alumina,   polishes,   electrical
insulators, and heat exchange media.

DESCRIPTION OF BAUXITE REFINING PROCESSES

Bauxite is the only ore of  aluminum  used  commercially  in  the
United   States.   Aluminum  production  is  unique  among  metal
manufacturing techniques  in  that  nearly  all  purification  is
accomplished  in  the  bauxite  refining process.  No significant
removal of impurities occurs during the subsequent  reduction  to
metal.

In the United States, bauxite is refined using the Bayer process.
The  classic Bayer process may be broadly divided into four major
operations:

 1. Bauxite grinding and digestion,
 2. Red mud removal and liquor purification,
 3. Precipitation and classification, and
                               519

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             BAUXITE REFINING SUBCATEGORY  SECT-III
digestion
       or
       or
  4.  Calcination.

 A variation of  the  process,  known  as   the   combination   process,
 allows additional alumina  recovery  from solid  residues when  high-
 silica bauxites are used as  the  raw material.

 Bauxite  refining   is   characteristically conducted  in very  large
 scale installations.   The  process is conducted in  an essentially
 closed circuit  with extensive  reuse and recycle of process water.
 Economic   considerations  make  the maximum recovery of  heat  and
 reagents  a  necessity.   Production processes  for  the  bauxite
 refining   subcategory  are  presented schematically  in Figure  III-l
 (page 527)  and  described in  detail  below.

 RAW  MATERIALS

 Bauxite  consists   of   hydrated   aluminum    oxide    and   various
 impurities,  including   iron  oxide,   titanium  dioxide,  silicon
 dioxide,  and compounds   of  phosphorus   and  vanadium.    A   basic
 distinction is made  between  monohydrate bauxite, which  contains
 alumina   in   the   form of  boehmite or diaspore    (A12O3   H2O),
 and    trihydrate  bauxite,   in the  form of   gibbsite
 or    A1(OH)3),    because    they require    different
 conditions.   Further  distinctions  of   ore type include   high
 low   silica  content,    high  or  low  iron content,  and fast-
 slow-settling red mud  after  digestion.

 BAUXITE GRINDING AND DIGESTION

 Bauxite  ore is  crushed  and wet-ground   with  a  caustic-rich
 solution   in preparation  for  the digestion  process.  The bauxite
 must  be ground  finely enough to ensure   effective  digestion  but
 not   so  finely that the red mud  residue presents  problems during
 settling  and filtration.   One  plant reports  the  use  of  scrubbers
 for dust  control in the  bauxite handling operations.  Because  the
 water   from  these scrubbers  is returned to the  process to recover
 the bauxite  value,  it is considered to  be a  process  water  stream
 rather  than  a wastewater stream.

 The   ground  bauxite slurry is  fed to digesters  where the hydrated
 alumina   in  the bauxite  is converted to a  soluble   salt,  sodium
 aluminate.   The  reaction is  accomplished   using  either  sodium
 hydroxide    or  a  combination  of  lime  and   sodium  carbonate.
 Wastewater from wet air  pollution control on lime  kilns  at   two
 plants  is   sent to the  digesters.  Because  the  scrubber effluent
 is returned  to  the process and not discharged,   it  is  considered
 to be a process water stream rather than a wastewater stream.

 Digestion    conditions   (temperature,    pressure,   and  caustic
 concentration)   depend   on   the   type   of   bauxite   processed.
Monohydrate   bauxites   require   temperatures  between  200   and
 250°C  at up to 35 atm   pressure.   Trihydrate  bauxites  can   be
digested  under  the more moderate conditions of 120 to 170°C and
 3 to 5 atm pressure.
                               520

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            BAUXITE REFINING SUBCATEGORY  SECT-III
The product of the  digestion  process  is  a  slurry  containing
sodium  aluminate  in  aqueous  solution  and undissolved solids.
This slurry enters a system of expansion vessels or "flash tanks"
for cooling, pressure reduction, and heat recovery.   The  stream
recovered from the expansion process is returned to the digesters
to  provide  some of the heat needed to maintain proper digestion
temperatures.  Condensate from the vapor is frequently  used  for
boiler  water.   At  one  plant  condensate  is  used for hydrate
washing.  Excess condensate or condensate which is unsuitable for
use in boilers may be disposed of.


RED MUD REMOVAL AND LIQUOR PURIFICATION

The digested bauxite suspension contains solid, insoluble bauxite
particles of various sizes and compositions in a sodium aluminate
solution..  Particles above a certain size, e.g., 100 microns, are
called  "sand"  and  may  include  undigested   bauxite,   quartz
particles,  or  common  sand.   Sand is usually removed from  the
suspension before red mud thickening.

The insoluble residue remaining in suspension after desanding  is
commonly  known  as  red  mud.   Red  mud  contains  iron oxides,
titanium  dioxide,  aluminum  present  with  silica,  and   other
secondary  impurities.   A  flocculating  agent  is  added to the
process suspension to  enhance  settling  of  the  fine  red  mud
particles.

The  overflow  from  the  mud  settling  and  thickening steps is
further clarified by  filtration.   This  step  removes  red  mud
particles from the supersaturated aluminate liquor.

The red mud settled from the process liquor is thickened, washed,
and  sometimes  filtered  to  recover caustic and alumina values.
The mud is then moved as a waterborne  slurry  to  a  waste  area
known as a red mud lake or impoundment for disposal.

.When high-silica bauxites such as those from Arkansas are used as
the   raw  material  for  alumina  production,  the  "combination
process" can be applied to  recover  alumina  and  sodium  values
which  would  otherwise  be lost in the red mud.  As much as one-
third of the total  alumina  value  produced  by  a  plant  using
Arkansas   bauxite   may   be   trapped   in   insoluble   sodium
aluminosilicates which are removed from the process with the  red
mud.

In  the  combination  process,  the  red  mud is treated first by
filtration to reduce the evaporative load and then  by  sintering
and  leaching  to  recover alumina.  After filtering and washing,
the remaining solid residue or "brown mud" is sent to a mud  lake
for  disposal.  The very pure filtrate, known as white liquor, is
either combined with  the  process  stream  or  precipitated  and
calcined separately to produce chemical-grade alumina.

Red  muds  from  various  bauxites have different characteristics
                               521

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            BAUXITE REPINING SUBCATEGORY  SECT-III
which produce differing disposal  considerations.   For  example,
the  yield  of  red  mud  residue  from  Surinam  bauxite  is low
(approximately 1/3 kkg per kkg of alumina product), and  the  mud
is  amenable  to  filtration  and  effective washing on a filter.
Thus, the final residue is relatively easy to handle and disposal
area requirements are moderate.  On the other hand, red muds from
Arkansas and Jamaican  bauxites  are  produced  in  much  greater
yield,  (approximately  2  kkg  and  1  kkg  per kkg of  alumina,
respectively), because of their larger content  of  contaminants.
The physical characteristics of Jamaican bauxite red mud are such
that  filtration  is difficult and countercurrent decantation may
be  required.   It  also  settles  poorly,  reaching   a   solids
concentration  of  only about 30 percent after normal settling as
compared to more than 50 percent solids for the muds  from  other
ores.  As a result, area requirements for these red mud lakes are
large.

One  company  which refines Jamaican bauxite has developed a sand
bed filtration technique.  In this technique, red mud  is  pumped
to  a  drying  bed  where  the solids concentration of the mud is
increased from 15 or 20 percent to more  than  50  percent.   The
surface  of  the  mud drying bed is kept dry by drawing water off
the top and, at one of the two plants using sand bed  filtration,
pumping it to a "clear lake." Underflow is also drawn out through
the  sandy  bottom  of the bed and sent to the clear lake.  Clear
lake water is then recycled to the  bauxite  refining  operations
for  use  as process water, forming a nearly-closed water system.
The second plant that practices sand bed filtration  of  red  mud
wastes  does  not  have a clear lake, practices no recycle of mud
lake water to the process, and  discharges  neutralized  effluent
directly to surface waters.

Of  the  alumina plants which do not practice sand bed filtration
of red mud, all report the use of red mud lakes.  In addition,  a
refinery  may  have  a  process  water lake for recycle of higher
quality water than is found in the mud lake  and  a  storm  water
lake  to collect large volumes of rainwater runoff from the plant
site.  Minor remaining storage  capacity  in  abandoned  red  mud
lakes  may  be utilized to dispose of small quantities of aqueous
wastes which are intolerable in the recycle circuit.  Examples of
such wastes are spent  acids  from  equipment  cleaning  and  the
effluent from salting-out evaporators.

PRECIPITATION AND CLASSIFICATION

The purified sodium aluminate solution obtained by removing solid
impurities   from   the   digested  liquor  passes  through  heat
exchangers and is  cooled  before  being  discharged  into  large
precipitation  vessels.  Vapor produced in the flash cooling area
is condensed and reused in other parts of the plant.

During precipitation, aluminum hydroxide  crystallizes  from  the
super-saturated   sodium   aluminate  in  the  presence  of  seed
crystals.   The precipitation conditions are carefully  controlled
so that the solids formed will be amenable to easy separation and
                               522

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            BAUXITE REPINING SUBCATEGORY  SECT-III
washing.   The  precipitated  hydrate  crystals are classified by
size; small crystals are washed and fed  to  calcining  furnaces.
Aluminum   trihydrate  scale  can  also  be  recovered  from  the
precipitators and processed to  make  an  activated  alumina  by-
product.

The  spent  liquor  separated  from  the  hydrate crystals during
classification  is  returned  to  the  grinding   and   digestion
processes  to recover the caustic value of the stream.  The spent
caustic is first heated in heat exchangers by the steam recovered
from  the  flash   cooling   of   the   process   liquor   before
precipitation.   The liquor then passes through evaporators which
remove excess water.  The caustic is thus  reconcentrated  before
being mixed with the bauxite ore in the digesters.

The vapor generated in the spent caustic evaporators is condensed
in   barometric  condensers  using  once-through  cooling  water.
Although occasional upsets may cause entrainment of caustic,  the
barometric  condensate,  also  referred  to as hotwell discharge,
from properly operated evaporators is generally  a  high  quality
water  which  is  either impounded with the red mud or discharged
directly to surface waters.

Some provision must be made to bleed off a part of  the  recycled
caustic  to  prevent  the  accumulation  of  soluble salts in the
system.  In some plants, one of the evaporators  is  a  "salting-
out"  evaporator  which  concentrates  a  portion of ,the recycled
caustic stream.  The concentrated stream is then disposed  of  in
an old mud lake or a landfill.

An alternate method of removing salts is to mix some of the spent
liquor   with   the  slurry  from  the  digesters.   The  soluble
contaminants are removed by the red mud which  is  then  filtered
out  and  discarded.   This  technique  of  salt removal has been
demonstrated in only one plant and may not be possible  with  red
mud from all bauxite ore types.

One plant removes soluble salts from the process by carbonating a
small  amount  of  pregnant liquor from the precipitation process
and some of the hydrate seed.  An alumina precipitate is  settled
from  the  carbonated mixture and calcined.  The recovered sodium
aluminate is then returned to  the  process  at  the  mixing  and
digestion  operation.   The  solution  from which the alumina was
precipitated  contains  neutralized  soluble  impurities  and  is
directly discharged without further treatment.

CALCINATION

The  moist  filter  cake of aluminum oxide from the precipitation
and classification operations is conveyed to calciners  where  it
is  converted  to  anhydrous  alumina, the form most suitable for
later use in electrolytic  reduction  to  aluminum  metal.   Dust
control   for   the   calciners   is  provided  by  electrostatic
precipitators or baghouse filters.
                               523

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            BAUXITE REFINING SUBCATEGORY  SECT-III
One plant dries part of  the  hydrate  filter  cake  rather  than
exposing  it  to  the more severe conditions of calcination.  The
product of this operation is sold as a dried hydrate.  Condensate
from the dryers is collected  and  reused  in  the  precipitation
process.

PROCESS WASTEWATER SOURCES

A  variety  of  processes  are involved in bauxite refining.  The
significant wastewater sources  that  are  associated  with  this
subcategory can be subdivided as follows:

 1. Digester condensate,
 2. Barometric condenser effluent,
 3. Carbonation plant effluent, and
 4. Mud impoundment effluent.

OTHER WASTEWATER SOURCES

There  are  other  waste  streams  associated  with  the  bauxite
refining subcategory.  These waste streams include, but  are  not
limited to:

 1. Stormwater other than that which falls within the
    process water impoundment area, and
 2. Maintenance and cleanup water.

These  waste  streams  are  not  considered  as  a  part  of this
rulemaking.  EPA believes that the flows and  pollutant  loadings
associated with these waste streams are insignificant relative to
the   waste   streams  selected,  or  are  best  handled  by  the
appropriate  permit  authority  on  a  case-by-case  basis  under
authority of Section 403 of the Clean Water Act.

AGE, PRODUCTION, AND PROCESS PROFILE

Figure   III-2  (page 529)  shows  the  location  of   the  eight
alumina  plants operating in the United  States.    This   figure
shows   that  the plants  are located in the southern states  and
in the U.S. Virgin Islands.

Table  III-l (page 524) summarizes the relative age and discharge
status   of the  eight alumina plants.   Most of the  plants  are
between 20 and 40 years old.  None of the alumina plants are more
than 50  years old.

Table   III-2 (page 525)  lists  the  1982  production ranges for
the alumina plants.   Four of the eight  plants  produce  200,000
to   300,000  kkg/yr   as   aluminum   contained.    Two   plants
produce less than 200,000 kkg/yr,  and the remaining two  produce
more  than  400,000 kkg/yr as aluminum contained.

Table   III-3  (page  526) lists the major  production  processes
associated  with the refining of bauxite.   Also shown   is   the
number   of   plants generating wastewater from these  processes.
                               524

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            BAUXITE REFINING SUBCATEGORY  SECT-III
                              Table III-l

        INITIAL OPERATING YEAR (RANGE)  SUMMARY OF PLANTS
      IN THE BAUXITE REFINING SUBCATEGORY BY DISCHARGE TYPE

        Initial Operating Year ^ Range  (Plant Age ^ years)
Type of
1982-
1963
1962-
1953
1952-
1943
1942-
1933
Discharge   (0-20)  (20-30) (30-40) (40-50)
    No. of Plants
Before
 1932
(<50)
                                        Total
Direct
Indirect
Zero
TOTAL
0
0
1
1
2
0
1
3
1
0
2
3
0
0
1
1
0
0
0
0
3
0
5
8
                           Table III-2
         PRODUCTION FOR THE BAUXITE REFINING SUBCATEGORY
                        Alumina Production1  (1982)
Type of
Discharge
Direct
Indirect
Zero
Total
0-200
0
0
2
2
200-300
3
0
1
4
300-400
0
0
0
0
400-600
0
0
2
2
Total
3
0
5
8
  In thousands kkg/yr of contained aluminum
                                525

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             BAUXITE REFINING SUBCATEGORY  SECT-III
                               Table III-3
            SUMMARY OF BAUXITE REFINING PROCESSES AND
                     ASSOCIATED WASTE STREAMS
         Process

 Bauxite grinding  and  digestion
    -Digester  condensate
 Red mud removal and liquor
    purification
    -Mud impoundment effluent
 Precipitation and classification
    -Barometric  condenser effluent
    - Carbonation plant effluent
Calcination
                                       No. Plants     No. Plants
                                          Process  with Wastewater
 8
 4
 8

 3
 8
 5
1
8
                                                       5
                                                       1
NOTE:  Through  reuse  or  evaporation  practices,
                      from a
                                                    a
                              526

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BAUXITE  REFINING SUBCATEGORY
SECT - III
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                      527

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BAUXITE REFINING SUBCATEGORY
SECT  - III
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BAUXITE REFINING SUBCATEGORY
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                   529

-------
BAUXITE REFINING SUBCATEGORY  SECT-III
  THIS PAGE  INTENTIONALLY LEFT BLANK
                 530

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            BAUXITE REFINING SUBCATEGORY   SECT-IV





                           SECTION IV

                        SUBCATEGORIZATION
This   section   summarizes   the factors considered  during  the
designation  of the bauxite refining subcategory and its  related
subdivisions.

FACTORS CONSIDERED IN SUBCATEGORIZATION

In   establishing   subcategories  in   the   nonferrous   metals
manufacturing   category,   the   following      factors     were
evaluated      for      use      in   determining     appropriate
subcategories.  These factore are discused more fully in  Section
IV of Vol. 1.

 1. Metal products, co-products, and by-products;
 2. Raw materials;
 3. Manufacturing processes;
 4. Product form;
 5. Plant location;
 6. Plant age;
 7. Plant size;
 8. Air pollution control methods;
 9. Meteorological conditions;
10. Treatment costs;
11. Nonwater quality aspects;
12. Number of employees;
13. Total energy requirements; and
14. Unique plant characteristics.

Evaluation of all factors that  could  warrant  subcategorization
resulted  in the designation of the bauxite refining subcategory.
Three factors were particularly important in  establishing  these
classifications:   the  type of metal produced, the nature of the
raw  materials used,  and the manufacturing  processes  involved.
Bauxite refining was considered as a  single  subcategory  during
the previous (1974) rulemaking  (40 CFR Part 421, Subpart A).

FACTORS CONSIDERED IN SUBDIVIDING THE BAUXITE REFINING
SUBCATEGORY

The rationale for considering further subdivision of the  bauxite
refining  subcategory into building blocks is based primarily  on
the production process used.    Within this subcategory, a number
of different operations are performed,   which  may  or  may  not
have   a  water  use  or discharge,   and  which  may require the
establishment  of  separate effluent limitations  and  standards.
While   bauxite   refining  is  still    considered    a    single
subcategory,   a   more   thorough examination of the  production
processes  has  illustrated  the   need  for   limitations    and
                               531

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            BAUXITE REFINING SUBCATEGORY   SECT-IV


standards based on a specific set of waste streams.   Limitations
and  standards will  be  based  on  specific flow allowances  for
the following subdivisions:

 1.  Digester condensate,

 2.  Barometric condenser effluent,

 3.  Carbonation plant effluent, and

 4.  Mud impoundment effluent.


OTHER FACTORS

Factors  other than manufacturing processes which were considered
in this evaluation either support the establishment of  the  four
subdivisions  or  were  determined  to be inappropriate bases for
subdivision.  Air pollution control methods, treatment costs, and
total  energy  requirements  are  functions   of   the   selected
subcategorization  factors,  namely metal product, raw materials,
and production processes.  Factors such as plant age, plant size,
and number of employees were also evaluated and determined to  be
inappropriate   bases   for   subdivision   of   this  nonferrous
metals subcategory.

TYPE OF PLANT

There is fundamentally only one process for refining bauxite: the
Bayer process.  The combination process, a variation of the Bayer
process,  further treats the red mud waste from the Bayer process
to  recover  additional  aluminum   and i  alkali   values.    The
differences in the manufacturing processes and wastes produced at
Bayer-process  plants  and  combination  process  plants  are not
significant enough to warrant further subdivision based on  plant
type.

RAW MATERIALS

The  major  process waste associated with the refining of bauxite
is the  red  mud  residue.   While  the  monohydrate  content  of
different   ores   requires  different  digestion  conditions  at
different plants, the  quality  of  the  red  mud  waste  is  not
significantly  affected.   Similarly,  the differences in quality
between the red mud from the Bayer  process  and  the  brown  mud
waste  generated  when  residues  from  high-silica  bauxites are
treated  by  the  combination  process  do  not  warrant  further
subdivision.

There  are  differences in the amount of mud generated per ton of
alumina produced which depend on the source of the bauxite.  Only
one-third ton of mud is produced per ton of alumina when  Surinam
bauxite  is  processed;  two or more tons of mud are produced per
ton of bauxite when Arkansas bauxite is  refined.   Nevertheless,
these differences affect the size, not the nature of the disposal


                               532

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            BAUXITE REFINING SUBCATEGORY   SECT-IV
problem.   Therefore,  the  specific type of bauxite raw material
refined is not chosen as a basis for further subdivision.

PLANT LOCATION

The relationship between annual rainfall and  annual  evaporation
is  significant  at  bauxite  refining plants because the process
facilities and red mud lakes typically cover  large  land  areas.
In  regions  where  precipitation  exceeds evaporation, collected
rainfall runoff can accumulate  and  present  disposal  problems.
However,  if provisions are made to segregate process wastewaters
and runoff from plant sites, the runoff can be discharged to  its
normal  water  course.  By allowing the discharge of net rainfall
from the impoundment areas, accumulation of water and  disruption
of  the plant's water balance can be avoided.  Therefore, further
subdivision based on plant location is not necessary.
                               533

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BAUXITE REPINING SUBCATEGORY   SECT-IV
   THIS PAGE INTENTIONALLY LEFT BLANK
                   534

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             BAUXITE REFINING SUBCATEGORY   SECT-V




                            SECTION V

            WATER USE AND WASTEWATER CHARACTERISTICS
This   section   describes  the  characteristics  of   wastewater
associated  with  the bauxite refining subcategory.  Data used to
quantify  wastewater  flow  and  pollutant   concentrations   are
presented,   summarized,  and  discussed.   The  contribution  of
specific production processes to the overall wastewater discharge
from bauxite refining plants is identified whenever possible.

The two  principal  data  sources were data collection portfolios
(dcp)  and field sampling results.  Data  collection  portfolios,
completed  for  each  of  the bauxite  refining  plants,  contain
information regarding wastewater flows and production levels.

In  order  to  quantify  the  pollutant  discharge  from  bauxite
refining  plants,  a  field  sampling  program   was   conducted.
Wastewater   samples   were   analyzed,  for  124   of   the   126
toxic  pollutants   and other  pollutants   deemed   appropriate.
(Because  the  analytical standard for TCDD was judged to be  too
hazardous  to  be made generally available,  samples  were  never
analyzed   for  this pollutant.    Also,   samples   were   never
analyzed  for asbestos.  There is no reason to expect  that  TCDD
or    asbestos    would   be  present    in   bauxite    refining
wastewater.)    Two   plants  were selected for sampling  in  the
bauxite   refining   subcategory.    A  complete   list   of  the
pollutants  considered  and a summary of the techniques  used  in
sampling and laboratory analyses are  included in  Section  V  of
the General Development Document.   In general,  the samples were
analyzed  for  three classes of   pollutants:   priority  organic
pollutants,     priority   metal   pollutants,    and    criteria
pollutants (which includes both conventional and  nonconventional
pollutants).

No    additional  sampling  was  performed  by   EPA    following
proposal. Therefore,  the  pollutant selection process  discussed
in Section IV  and  the  compliance cost  and  pollutant  removal
estimates presented  in  Section  X  are based on the same   data
used   for  proposal.    EPA   received   several  comments  from
industry   which provided additional wastewater  characterization
data.   These  data  were   used   to  help  EPA  formulate   its
recommendations  for  this subcategory.

As  described  in  Section  IV  of  this  supplement, the bauxite
refining  subcategory  has  been  further   divided   into   four
building  blocks.   Differences    in   the  characteristics   of
the wastewater streams corresponding to each subdivision  are  to
be  expected  and  are  addressed  separately in the  discussions
that follow.  These wastewater sources are:

1. Digester condensate,
                               535

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              BAUXITE REFINING SUBCATEGORY   SECT-V
 2. Barometric condenser effluent,

 3. Carbonation plant effluent,  and

 4. Mud impoundment effluent.

 WASTEWATER CHARACTERISTICS DATA

 Data used to characterize the various  wastewaters  associated with
 bauxite  refining  come  from  two  sources:     data    collection
 portfolios (dcp)  and analytical data from field  sampling  trips.

 DATA COLLECTION PORTFOLIOS

 In  the data collection portfolios,  plants were  asked  to  indicate
 which  of the priority  pollutants  were known  or  were believed to
 be  present  in  their   effluent.    Two   plants  indicated   that
 priority  organics  were known  to  be   present.    Three   plants
 stated   that priority  metals  were  known or   believed   to  be
 present in their  effluent.  The responses from the three  plants
 which  provided information are summarized below.
      Pollutant

   23. chloroform
   44. methylene chloride
   48. dichlorobromomethane
   65. phenol
   68. di-n-butyl phthalate
   70. diethyl phthalate
   86. toluene
 114. antimony
 115. arsenic
 117. beryllium
 118. cadmium
 119. chromium (Total)
 120. copper
 121. cyanide (Total)
 122. lead
 123. mercury
 124. nickel
 125. selenium
 126. silver
 127. thallium
 128. zinc

FIELD SAMPLING DATA
Known Present

      1
      1
      1
      2
      1
      1
      1
      2
      2
      1
      1
      2
      2
      1
      2
      2
      1
      2
      2
      1
      2
Believed Present

       0
       0
       0
       2
       0
       0
       0
       2
       3
       1
       2
       3
       3
       0
       3
       3
       2
       3
       3
       2
       3
In  order to quantify the concentrations of pollutants present in
wastewater from bauxite refining plants, wastewater samples  were
collected  at  two  of the eight plants.  Diagrams indicating the
sampling sites and contributing production processes are shown in
Figures  V-l  and  V-2  (pages 552 to 553).
                               536

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             BAUXITE REFINING SUBCATEGORY   SECT-V
The sampling  data  for  the  bauxite  refining  subcategory  are
presented in tables at the end of this section.  The stream codes
listed  may  be  used  to  identify  the  location of each of the
samples on the process flow diagrams  in  Figures  V-l  and  V-2.
Where  no  data  are  listed  for a specific day of sampling, the
wastewater samples for the stream were not collected.

Several points regarding these tables should  be  noted.   First,
the  data  tables include some samples measured at concentrations
considered not quantifiable.  The base-neutral extractable,  acid
extractable,  and  volatile organics are generally considered not
quantifiable at concentrations equal to or less than 0.010  mg/1.
Below  this  concentration,  organic  analytical  results are not
quantitatively accurate; however,  the  analyses  are  useful  to
indicate  the  presence of a particular pollutant.  The pesticide
fraction is considered not quantifiable at  concentrations  equal
to   or  less  than  0.005  mg/1.   Nonquantifiable  results  are
designated in the tables with an asterisk  (double  asterisk  for
pesticides).

Second, the detection limits shown on the data tables are not the
same  in  all  cases  as the published detection limits for these
pollutants by the same analytical methods.  The detection  limits
used  were  reported  with  the analytical data and hence are the
appropriate  limits  to  apply  to  the  data.   Detection  limit
variation  can  occur  as  a  result  of  a number of laboratory-
specific,   equipment^specific,   and   daily   operator-specific
factors.   These  factors  can  include day-to-day differences in
machine calibration, variation in stock solutions, and  variation
in operators.

Third,  the  statistical  analysis  of data includes some samples
measured   at  concentrations  considered    not    quantifiable.
Priority  organics  data reported as an asterisk or with a  "less
than"  sign  are  considered as detected but  below  quantifiable
concentrations,  and  a value of zero is used for  averaging.   A
value  of  zero  is also  used  for  averaging  if  a   pollutant
is   reported as not detected.   Finally,  priority metal  values
reported as  less  than  a certain value were considered as below
quantification  and a value of zero is used in the calculation of
the average.

Finally,  appropriate  source  water concentrations are presented
with the sampling data.  The method  by  which  each  sample  was
collected is indicated by number as follows:
    One-time grab
    Manual composite during intermittent process operation
    8-hour manual composite
    8-hour automatic composite
    24-hour manual composite
WASTEWATER CHARACTERISTICS AND FLOWS BY BUILDING BLOCK
                               537

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             BAUXITE REFINING SUBCATEGORY   SECT-V
Bauxite  refining  involves four principal sources of wastewater,
each of which has  potentially  different  characteristics.   The
wastewater   characteristics  corresponding  to  each   will   be
described separately in the discussions that follow. A  discharge
is  allowed from the overflow of a process wastewater impoundment
in  a  volume equal to the difference between  the  precipitation
that  falls  within  the impoundment   in  a given month and  the
evaporation   from   that  impoundment   (this  is  termed    net
precipitation).        EPA      is   not     promulgating     any
modifications   to   the  no   discharge limitation  for  process
wastewater pollutants (which was originally promulgated April  8,
1974).   For this reason, water  use  and   discharge flow   will
be   addressed   only   with regard   to  the  net  precipitation
discharge from mud  impoundments in the discussions that follow.

DIGESTER CONDENSATE

Bauxite ore is digested with  caustic  to  produce  a  slurry  of
sodium  aluminate  in  aqueous  solution with undissolved solids.
This slurry enters a system of expansion vessels or "flash tanks"
for  cooling,  pressure  reduction,  and  heat  recovery.   Vapor
released  in the flash tanks is condensed as a high quality water
suitable for reuse as boiler water or product  wash  water.   The
digester  condensate is characterized by treatable concentrations
of phenols, low concentrations of suspended solids, and high  pH.
Sampling  data for the digester condensate are presented in Table
V-2 (page 541).

BAROMETRIC CONDENSER EFFLUENT

The spent liquor  separated  from  the  hydrate  crystals  during
classification   is   returned  to  the  grinding  and  digestion
processes to recover the caustic value of the stream.  The liquor
passes through evaporators which  remove  excess  water  and  re-
concentrate the caustic stream for reuse.

The vapor generated in the spent caustic evaporators is condensed
in  barometric  condensers.  Although occasional upsets may cause
entrainment of caustic,  the  condensate,  also  referred  to  as
hotwell  discharge,  is  a good quality, somewhat alkaline water.
This stream  is  characterized  by  treatable  concentrations  of
phenols  and  suspended  solids.   Sampling  data  for barometric
condenser effluent are presented in Table V-3 (page 544).

CARBONATION PLANT EFFLUENT

Some provision must be made to  remove  soluble  salts  from  the
recycled caustic to prevent the accumulation of impurities in the
process.  One plant removes and carbonates a small portion of the
process  liquor  and  the  hydrate  seed.   The resulting alumina
precipitate is returned to the digesters.  The overflow from  the
carbonation   process   contains  the  soluble  impurities  in  a
neutralized  solution  which  is   characterized   by   treatable
concentrations  of  phenols  and suspended solids.  Sampling data
                               538

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             BAUXITE REFINING SUBCATEGORY   SECT-V
for  carbonation plant effluent are presented in Table V-4  (page
547).

MUD IMPOUNDMENT EFFLUENT

Red mud is the major waste stream from the bauxite refinery.   It
contains  all  of  the  impurities from the bauxite, such as iron
oxide, silicon dioxide, and titanium  dioxide,  as  well  as  by-
products  formed  during  the  process,  such  as sodium aluminum
silicates and calcium silicates.  Red mud is discharged to ponds,
along  with  other  process  streams,  where  insoluble   solids,
including   the  oxides  of  metallic  elements,  settle  out  of
suspension.  The clarified  liquid,  characterized  by  treatable
concentrations  of  phenols  and  high  pH,  can  be recycled and
reused  directly  from the mud lake or  decanted  to   a   "clear
lake"  before discharge in accordance with the net  precipitation
limitations.

The  water  use and discharge rates of this wastewater are listed
in Table V-l (page 540) in liters per  year  of  mud  impoundment
effluent.   Sampling    data   for   the   effluent   from    mud
impoundments at two plants are presented in Table V-5 (page 549).
At  plant A,   the  impoundment effluent is  discharged  directly
from  the mud lake without recycle to  the process.   At plant B,
overflow and underflow from the red mud drying beds are sent to a
clear  lake  from  which  water  is recycled or discharged.
                               539

-------
BAUXITE REPINING SUBCATEGORY   SECT-V
                  Table V-l


   WATER USE AND DISCHARGE RATES FOR
    MUD IMPOUNDMENT EFFLUENT (1/yr)
  Plant Code

       1171

       1141

       1076

       1136

       1073

       1135

       1032

       1015
Discharge Flow

       1.45 x 109

       5.95 x 109

       2.983 x 108

       0

       0

       0

       0

       0
                 540

-------
             BAUXITE REPINING SUBCATEGORY   SECT-V
                            TABLE V-2

                  BAUXITE REFINING SUBCATEGORY
                DIGESTER CONDENSATE SAMPLING DATA
           Pollutant
Toxic Pollutants
Stream Sample   Concentration  (mg/1)
 Code   Type  Source  Day _!  Day 2^  Da
1.

4.
6.
11.
21.
22.
23.

24.
31.
34.

39.

44.

55.

57.

58.
59.
60.

64.

65.

66.

67.
68.

70.

71.
acenaphthene

benzene
carbon tetrachloride
1,1,1-trichloroe thane
2,4, 6-tr ichlorophenol
parachlorometacresol
chloroform

2-chlorophenol
2 , 4-dichlorophertol
2 , 4-dimethylphenol

fluoranthene

methylene chloride

napthalene

2-nitrophenol

4- nitrophenol
2,4-dinitrophenol
4 , 6-dini tro-o-cresol

pentachlorophenol

phenol

bis( 2-ethylhexyl) phthalate

butyl benzyl phthalate
di-n-butyl phthalate

diethyl phthalate

dimethyl phthalate
101
201
201
101
201
201
201
101
201
201
201
101
201
101
201
101
201
101
201
101
201
201
201
101
201
101
201
101
201
101
201
101
101
201
101
201
101
5
5
1
1
1
5
5
1
1
5
5
5
5
5
5
1
1
5
5
5
5
5
5
5
5
5
5
5
5
5
5
5
5
5
5
5
5





ND
ND
*
*
ND
ND

*
*

*




ND
ND
ND

*

ND
*
ND
0.790
0.020
*
*




0.018

*


0.032
ND
*
0.054
ND
0.011

ND
0.015
*
*
0.073
0.039


ND
ND
ND

0.016

ND
1.800
2.100
0.066
0.053
*
0.034

0.015
0.080
0.022
0.026
0.093
0.140
0.140



*
0.093


0.930
0.420
*
*
0.018
0.020
0.018
0.130

*






2.300
1.30
0.055

*
*
0.047
0.016
0.280
0.038
0.
0.
0.




*
0.


0.

0.
*
0.
0.
0.
*
*
0.


0.

*

1.
0.
0.
0.
*
*
0.
*
0.

                               541

-------
              BAUXITE REFINING SUBCATEGORY   SECT-V
                       TABLE V-2 (Continued)

                   BAUXITE REFINING SUBCATEGORY
                 DIGESTER CONDENSATE SAMPLING DATA
            Pollutant
 Toxic Pollutants
  73. benzo (a)pyrene

  76. chrysene

  77. acenapthylene


  80. fluorene
  84. pyrene

  85. tetrachlorethylene


  86. toluene

  87. trichloroethylene

  89. aldrin

  92. 4,4'-DDT

  93. 4/4'-DDE(p,p'DDX)

  94. 4,4'-DDD(p,p'TDE)*

  97. endosulfan  sulfate

  98.  endrin
  99.  endrin aldehyde


101.  heptachlor  epoxide

102.  alpha-BHC
104.  gamma-BHC


105.  delta-BHC
106.  PCB-1242 (Arochlor 1242)

107.  PCB-1254 (Arochlor 1254)


108. PCB-1221 (Arochlor 1221)

109. PCB-1232 (Arochlor 1232)
Stream Sample   Concentration  (mg/1)
 Code   Tvoe  Source  Dav 1  Dav 2  n.
101
• - 201
101
201
101
201
101
101
201
101
201
101
201
101
201
201
101
201
101
201
101
101
201
201
101
201
101
201
101
101
201
201
101
201
101
201
101
201
101
201
• • i
5
5
5
5
5
5
5
5
1
1
1
1
1
1
5
5
5
5
5
5
5
5
5
5
5
5
5
5
5
5
5
5
5
5
5
5
5
5
5














**
**
**
**
**





**
**
**

**
**

**
**
**
**
**
**
**
**



0.030

*
*
*

0.012

0.053
*

**
**
**
**
**


**
**
**
**
**
**

**
**
**
**
**
**
**
**
**
**
**


*

0.053
0.033
*
*
*
*
0.029
0.345
*
*

**
**

**

**
**
**
**
**

**


**


**

**
**
**

**
*
*
*


0.

*
*

0.
0.

*

*
*

*
*
*

*

*
*
*
*
*
*

*
*
*
*
*
*
*
*
                               542

-------
             BAUXITE REFINING SUBCATEGORY   SECT-V
                      TABLE V-2 (Continued)

                  BAUXITE REFINING SUBCATEGORY
                DIGESTER CONDENSATE SAMPLING DATA
           Pollutant
Toxic Pollutants
110. PCB-1248 (Arochlor 1248)
111. PCB-1260 (Arochlor 1260)

112. PCB-1016 (Arochlor 1016)


114. antimony

115. arsenic

121. cyanide (Total)


125. selenium

126. silver

127. thallium


Nonconventional Pollutants

Chemical oxygen demand (COD)

chloride

fluoride
phenols (4-AAP)


Conventional Pollutants

oil and grease

total suspended solids (TSS)

pH  (std. units)
Stream Sample   Concentration  (mg/1)
 Code   Type  Source  Day 1  Day 2  Da
                „       .  _      _  __
101
201
101
201
101
201
101
201
101
201
101
201
101
201
101
201
101
201
5
5
5
5
5
5
5
5
5
1
1
5
5
5
5
5
5
**
**
**
**
**
**
<0 . 1
<0
<0
<0


<0
<0
<0
<0
<0
<0
.1
.01
.01


.01
.01
.2
.2
.1
.1
**
**
**
**
**
**

-------
             BAUXITE REFINING SUBCATEGORY   SECT-V
                            TABLE V-3

                  BAUXITE REFINING SUBCATEGORY
            BAROMETRIC CONDENSER (HOT WELL) DISCHARGE
                  RAW WASTEWATER SAMPLING DATA
           Pollutant
Toxic Pollutants
Stream Sample   Concentration  (mg/1)
 Code   Type  Source  Day 1^  Day 2.  Da
1.

4.
10.
20.
21.
22.

23.

24.
31.
34.

39.

44.

55.
57.

58.
59.
60.
64.
65.

66.

67.

68.

70.

71.

acenaphthene

benzene
l,2,dichloroethane
2-chloronaphthalene
2,4, 6-tr ichlorophenol
parachlorometacresol

chloroform

2-chlorophenol
2 , 4-dichlorophenol
2 , 4-dimethylphenol

fluoranthene

methylene chloride

napthalene
2-nitrophenol

4- nitrophenol
2 , 4-dini trophenol
4 , 6-dinitro-o-cresol
pentachlorophenol
phenol

bis ( 2-e thy Ihexy 1 ) phthalate

butyl benzyl phthalate

di-n-butyl phthalate

diethyl phthalate

dimethyl phthalate

102
202
202
102
202
202
102
202
102
202
202
202
102
202
102
202
102
202
202
102
202
201
202
202
202
102
202
102
202
102
202
102
202
101
201
102
202
5
6
1
1
6
6
5
6
1
1
6
6
5
6
5
6
1
1
6
5
6
5
6
6
6
5
6
5
6
5
6
5
6
5
6
5
6
* *
* *
* * *
* *
*
ND 0.032
0.013
ND ND
* * 0.
* * * *
ND *
* 0.010
0.038
*
* * f *
*
* 0.063 0.
0.110 *
*
0.110 *
* *
ND ND *
ND ND
* 0.019
ND ND
* 0.075
ND 2.0 * *
0.790 0.170 0.016 0.
0.020 * 1.3 0.
* * *
*
* * *
* 0.016 *
* *
* *
*
0.011 *
                               544

-------
             BAUXITE REFINING SUBCATEGORY   SECT-V
                            TABLE V-3

                  BAUXITE REFINING SUBCATEGORY
            BAROMETRIC CONDENSER (HOT WELL) DISCHARGE
                  RAW WASTEWATER SAMPLING DATA
           Pollutant
Toxic Pollutants
 73. benzo (a)pyrene
 76. chrysene
 77. acenapthylene
 80. fluorene

 84. pyrene

 85. tetrachlorethylene


 86. toluene

 89. aldrin
 90. dieldrin


 91. chlorodane

 92. 4,4'-DDT

 93. 4,4'-DDE(p,p'DDX)


 94. 4,4'-DDD(p,p'TDE)*


 -97. endosulfan sulfate

 98. endrin

 99. endrin aldehyde

100. heptachlor

101. heptachlor epoxide

102. alpha-BHC


103. beta-BHC

104. gamma-BHC

105. delta-BHC
Stream
Code
102
202
102
201
102
202
202
202
102
202
102
202
202
102
202
102
202
102
202
101
202
102
202
102
202
102
202
202
102
202
101
201
102
202
102
202
102
202
202
Sample
Type
5
6
5
6
5
6
6
5
1
1
1
3.
6
5
6
5
6
5
6
5
5
5
6
5
6
5
6
6
5
6
5
5
5
6
5
6
5
6
6
Concentration
Source





*






**
**

**
**
**
**
**





**

**


**
**

**
**
**
**
**
**
Day 1 I








*

*

**



**

**



**

**

**
**

**

**

**

**

**
**
(mg/1)

)ay 2 Da


*
*
*

*




*
**
**
**
**
**
**
**
**

**
**
**
**

**

**
**
**
**


**
**
**
**
**
*
*
*
*
*
*
*


*
*

*
*
*
*
*
*
*
*
*



*
*
*

*
*
*
*
*
*
*
*
*
*
*
                               545

-------
BAUXITE REFINING SUBCATEGORY SECT-V
TABLE V-3 (Continued)
BAUXITE REFINING SUBCATEGORY
BAROMETRIC CONDENSER
RAW WASTEWATER
(HOT WELL)
DISCHARGE

SAMPLING DATA
Pollutant Stream Sample
Toxic Pollutants
106. PCB-1242 (Arochlor 1242)

107. PCB-1254 (Arochlor 1254)

108. PCB-1221 (Arochlor 1221)

109. PCB-1232 (Arochlor 1232)

110. PCB-1248 (Arochlor 1248)

111. PCB-1260 (Arochlor 1260)

112. PCB-1016 (Arochlor 1016)

121. cyanide (Total)

Nonconventional Pollutants
Chemical oxygen demand (COD)
chloride
fluoride
phenols (4-AAP)
Conventional Pollutants
oil and grease

total suspended solids (TSS)
pH (std. units)

Code Type
102 5
202 6
102 5
202 6
102 5
202 6
102 5
202 6
102 5
202 6
102 5
202 6
102 5
202 6
101 1
201 1

102 5
202 6
102 5
101 5
101 1
201 1

101 1
201 1
101 5
101 5
101 5
201 5
Concentration (mg/1)
Source Day 1
**
** **
**
** **
**
** **
**
** **
**
** **
**
** **
**
** **



39 36
24 31


ND 0.374
ND 0.020

ND 10
ND 5
768 373
277 296
8.70
8.0
Day 2 Da
— j^jT — — 37
•ft Is *
** *
** *
** *
** *
* * *
** *
** *
** *
** *
** *
** *
** *
* * *



36 50
28 30
20
0.
0.190 0.
0.023

9 2
4 4
275 270
462 291
9.12 9.
8.2
NOTES:
Sample type code
    1 - One time Grab
    5 - 24-hour manual composite
    6 - 24-hour automatic composite
 * Less than 0.01 mg/1
**Less than 0.005 mg/1

(a), (b) - Reported together
                               546

-------
             BAUXITE REPINING SUBCATEGORY   SECT-V
                            TABLE V-4
                  BAUXITE REFINING SUBCATEGORY
                   CARBONATION PLANT EFFLUENT
                  RAW WASTEWATER SAMPLING DATA
           Pollutant
Toxic Pollutants
21. 2,4, 6-trichldrophenol
22. parachlorometacresol
23. chloroform
24. 2-chlorophenol
31. 2, 4-dichlorophenol
34. 2,4-dimethylphenol
39. fluoranthene
44. methylene chloride
57. 2-nitrophenol
58. 4- nitrophenol
59. 2,4-dinitrophenol
60. 4,6-dinitro-o-cresol
64. pentachlorophenol
65. phenol
66. bis(2-ethylhexyl)phthalate
67. butyl benzyl phthalate
68. di-n-butyl phthalate
70. diethyl phthalate
71. dimethyl phthalate
77. acenapthylene
84. pyrene
85. tetrachlorethylene
87. trichloroethylene
89. aldrin
90. dieldrin
91. chlorodane
93. 4, 4'-DDE(p/p'DDX)
96. beta-endosulfan
97. endosulfan sulfate
100. heptachlor
101. heptachlor epoxide
103. beta-BHC
104. gamma-BHC
201
201
203
203
203
203
203
203
203
203
203
203
203
203
203
203
203
203
203
203
203
203
203
203
203
203
203
203
203
203
203
203
203
Stream Sample   Concentration  (mg/1)
 Code   Type  Source  Day 1^  Day .2  Da
201
201
203
203
203
203
203
203
203
203
203
203
203
203
203
203
203
203
203
203
203
203
203
5
5
1
5
5
5
5
1
5
5
5
5
5
5
5
5
5
5
5
5
5
1
1
ND
ND
*
ND
ND
*


ND
ND
ND
*
ND
ND
0.020



0.011




ND
ND
*
1.600
ND
ND


ND
ND
ND
ND
ND
2.100











0.054


0.140
*
*




1.300
0.016

*
*
0.017
0.130
*
*
0.021
*
                                               **
203
203
203
203
203
203
203
203
203
5
5
5
5
5
5
5
5
5

**
**


**
**
**
**
                                                             **

                                                             **
                                                             **
                                                             **

                                                             **
                                                             **
                                                             **

                                                             **
                                                             **
                                                             **
                               547

-------
             BAUXITE REFINING SUBCATEGORY   SECT-V
                            TABLE V-4

              BAUXITE REFINING DIGESTER CONDENSATE
                          SAMPLING DATA
           Pollutant
Toxic Pollutants
105. delta-BHC                  203     5
106. PCB-1242 (Arochlor 1242) a 203     5
107. PCB-1254 (Arochlor 1254) a 203     5

108. PCB-1221 (Arochlor 1221) a 203     5
109. PCB-1232 (Arochlor 1232) b 203     5
110. PCB-1248 (Arochlor 1248) b 203     5

111. PCB-1260 (Arochlor 1260) b 203     5
112. PCB-1016 (Arochlor 1016) b 203     5

114. antimony                   203     5
115. arsenic                    203     5
121. cyanide (Total)            203     1

125. selenium                   203     5
126. silver                     203     5
127. thallium                   203     5

Nonconventional Pollutants

Chemical oxygen demand (COD)    203     5
phenols (4-AAP)                  203     5

Conventional Pollutants

oil and grease                  203     1
total suspended solids (TSS)    203     5
pH (std. units)                  203     5
Stream Sample   Concentration
 Code   Type  Source  Day 1^
                **
                **
                **

                **
                **
                **

                **
                **
<0.01
                 (mg/1)
                	 2  Da
                **
                **
                **

                **
                **
                **

                **
                **
                      0.44
                     
-------
             BAUXITE REFINING SUBCATEGORY   SECT-V
                            TABLE V-5

                  BAUXITE REFINING SUBCATEGORY
                       MUD LAKE DISCHARGE
                  RAW WASTEWATER SAMPLING DATA
           Pollutant
Toxic Pollutants
Stream Sample   Concentration  (mg/1)
 Code   Type  Source  Day !_  Day 2!  Da
1.
6.
10.
21.

22.
23.

24.
31.

34.

39.

44.

48.
55.
57.

58.

59.
60.
64.

65.

66.

67.

68.

70.
71.

acenaphthene
carbon tetrachloride
1 , 2-dichlorethane
2,4, 6-tr ichlorophenol

parachlorometacresol
chloroform

2-chlorophenol
2 r 4-dichlorophenol

2 , 4-dimethylphenol

fluoranthene

methylene chloride

dichlorobromome thane
napthalene
2-nitrophenol

4- nitrophenol

2 , 4-dini.trophenol
4,6-dinitro-o-cresol
pentachlorophenol

phenol

bis(2-ethylhexyl)phthalate

butyl benzyl phthalate

di-n-butyl phthalate

diethyl phthalate
dimethyl phthalate

101
201
104
104
204
204
104
204
204
104
204
104
204
104
204
104
204
204
204
104
204
104
204
204
204
104
204
104
204
104
204
104
204
104
204
204
104
204
5
1
1
5
6
1
1
1
6
5
6
5
6
5
6
1
1
1
6
5
6
5
6
4
4
5
6
5
6
5
6
5
6
5
6
5
5
6
*
*
ND *
ND ND
* 0.026
*
ND 0.065
0.050
*

* *
*
*
* 0.051




ND ND

ND ND
ND ND
* 0.011

ND ND
* 0.034
ND 0.320
0.790 0.150
0.020 0.720
* *

* *
* *
0.011


0.048
0.054

*
0.015

0.047
0.060
*


*
*
0.020
*
*

0.067
0.040
0.310




0.035
0.230
0.330
0.650
*
*
*
*
0.010


0.


N
0.
0.
0.

*

*
*

0.

0.
*

0.



*

0.
0.
*
*
*
*
*
*
0.
*
1.
                               549

-------
BAUXITE REPINING SUBCATEGORY SECT-V
TABLE V-5
BAUXITE REFINING SUBCATEGORY
MUD LAKE DISCHARGE
RAW WASTEWATER SAMPLING DATA

Pollutant
Toxic Pollutants
77.

80.
84.

85.
86.
91.

92.

93.
95.
96.
97.

98.

99.
100.

101.

102

103.

104.

106.

107.

108.

109.

110.

acenapthylene

f luorene
pyrene

tetrachlorethylene
toluene
Cholordane

4,4' -DDT

4,4'-DDE(p,p'DDX)
alpha-endosulfan
beta-endosulfan
endosulfan sulfate

endrin

endrin aldehyde
heptachlor

heptachlor epoxide

alpha-BHC

beta-BHC

gamma-BHC

PCB-1242 (Arochlor 1242)

PCB-1254 (Arochlor 1254)

PCB-1221 (Arochlor 1221)

PCB-1232 (Arochlor 1232)

PCB-1248 (Arochlor 1248)

Stream
Code
104
204
104
104
204
104
204
201
204
104
204
204
104
104
104
204
104
204
204
104
204
104
204
104
204
104
204
101
204
a 101
204
a 101
204
a 104
204
b 104
204
b 104
204
Sample
Type
5
6
5
5
6
1
1
5
6
5
6
6
5
5
5
6
5
6
6
5
6
5
6
5
6
5
6
5
6
5
6
5
6
5
6
5
6
5
6
Concentration (mg/1)
Source



*



**
**
**
**
**




**

**
**
**
**
**

**
**
**
**
**
**
**
**
**
**
**
**
**
**
**
Day 1
*



*
0.012


**
**
**
**



**
**
**
**
**
**
**
**
**
**
**
**
**
**
**
**
**
**
**
**
**
**
**
**
Day 2




*

*
**
**
**
**

**
**
**
**

**

**
**
**
**

**
**
**

**
**
**
**
**
**
**
**
**
**
**
Da
0.
0.
*
*
*


*
*
*
*

*
*
*
*

*

*
*
*
*


*
*

*

*

*

*

*

*
550

-------
             BAUXITE REFINING SUBCATEGORY   SECT-V
                      TABLE V-5 (Continued)

                  BAUXITE REFINING SUBCATEGORY
                       MUD LAKE DISCHARGE
                  RAW WASTEWATER SAMPLING DATA
           Pollutant
Toxic Pollutants
Stream Sample   Concentration  (mg/1)
 Code   Type  Source  Day !_  Day 2^  Da
111. PCB-1260 (Arochlor 1260) b 104
                                204
112. PCB-1016 (Arochlor 1016) b 104
114. antimony

115. arsenic

121. cyanide (Total)


125. selenium

126. silver

127. thallium


Nonconventional Pollutants

Chemical oxygen demand (COD)

chloride

fluoride

phenols (4-AAP)


Conventional Pollutants

oil and grease

total suspended solids (TSS)

pH  (std. units)
104
204
104
204
104
204
104
204
104
204
104
204
104
204
104
204
5
6
5
6
5
6
5
6
1
1
5
6
5
6
5
6


<0
<0
<0
<0


<0
<0
<0
<0
<0
<0
**
**
**
**
.1
.1
.01
.01


.01
.01
.02
.02
.1
.1


<0
<0
0
0
0
<0
<0
<0
<0
<0
<0
<0
**
**
**
**
.1
.1
.2
.32
.01
.001
.01
.01
.02
.02
.1
.1
**
**
**
**
<0.1
<0 .1
0.14
0.08
0.003
<0.001
<0.01
<0.01
<0.02
<0 . 02
<0.1
<0 . 1
*
*
<0.

0.

0.
<0.
<0.

<0.

<0.
<0.
 101
 201
 101

 101
 201
 101
 201
 101
 201
 101
 101
 101
 201
5
5
5

5
5
5
5
1
1
5
5
5
5
 39
 24
364
977
374
943
451
495
 33
768
277
2
0
0

15
18
11
11
11

.197
.981




.70
.55

0
1
23
6
16
2
11
11

.116
.15




.76
.5

0
1
5
22
9
4
11

NOTES:
Sample type code
    1 - One time Grab
    2 - 24-hour manual composite
       * Less than 0.01 mg/1
      ** Less than 0.005 mg/1
      (a) or (b) - Reported together
                               551

-------
BAUXITE REFINING SUBCATEGORY
SECT - V
           
-------
BAUXITE  REFINING SUBCATEGORY
                                  SECT  - V
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-------
BAUXITE DEFINING SUBCATEGORY   SECT-V
       THIS PAGE INTENTIONALLY LEFT BLANK
                  554

-------
              BAUXITE REFINING SUBCATEGORY   SECT-VI



                           SECTION VI

                SELECTION OP POLLUTANT PARAMETERS
Section V of this supplement presented data from bauxite refining
plant  sampling  visits  and  subsequent chemical analyses.  This
section  examines  that  data  and  discusses  the  selection  or
exclusion  of  pollutants  for  potential  limitation.

This   section   discusses  the  selection  of  conventional  and
nonconventional pollutants for consideration for regulation.  The
discussion that follows also  describes  the  analysis  that  was
performed   to   select   or  exclude   priority  pollutants  for
further consideration for limitations and standards.   Generally,
pollutants  will   be  selected  for  further  consideration   if
they    are  present    in   concentrations  treatable   by   the
technologies  considered   in   this  analysis.    The
concentrations  used  for the toxic metals  are  the
treatment   performance  concentrations achievable
precipitation,      sedimentation,     and  filtration
The    concentrations    for    the   toxic  organics
long-term  performance
adsorption.
                                treatable
                                long-term
                               by    lime
                                 (L,S&F).
                                 are  the
values achievable  by  activated   carbon
CONVENTIONAL AND NONCONVENTIONAL POLLUTANT PARAMETERS

This  study  considered  samples  from   the   bauxite   refining
subcategory  for three conventional pollutant parameters (oil and
grease, total suspended solids, and pH) and  two  nonconventional
pollutant   parameters   (chemical   oxygen   demand   and  total
phenolics).  Because existing BPT regulations (40 CFR  Part  421,
Subpart   A)   specify   zero  discharge  of  process  wastewater
pollutants,    only   sampling   data    from    allowable    net
precipitation  discharges from mud  impoundments were  considered
in  the selection of conventional and  nonconventional  pollutant
parameters for regulation.

CONVENTIONAL AND NONCONVENTIONAL POLLUTANT PARAMETERS SELECTED

The conventional  and  nonconventional  pollutants  or  pollutant
parameters  selected  for  consideration  for  limitation in this
subcategory are pH and phenols.

The pH values observed in five samples ranged from 11.5 to 11.76.
Effective   and  consistent  removal  of  priority  organics   by
activated  carbon   or  chemical   oxidation   requires   careful
control of pH.  Therefore,, pH is selected for  consideration  for
limitation  in this subcategory.

Phenols  concentrations in six samples ranged from 0..116 to  1.23
                               555

-------
              BAUXITE REFINING SUBCATEGORY   SECT-VI
rag/1.   The  observed  concentrations  are above those considered
treatable by identified treatment technology.  Sampling data from
process wastewater streams, presented in Section V, indicate  the
presence  of  phenolic  compounds throughout the bauxite refining
process.   Therefore, phenols are considered for  limitation   in
this subcategory.

The  major  source  of  oil  and  grease  in the bauxite refining
subcategory  is  from  the  lubrication  of  process   machinery.
Because  oil  and  grease in process wastewater is not present in
significant concentrations, oil and grease is  not  selected  for
limitation.

Total  suspended solids (TSS) concentrations in six samples range
from 2 to 18 mg/1.  Although treatable, these concentrations  are
not  considered  to  be  significant  and  are  not  expected  to
interfere  with  end-of-pipe  treatment  technologies   such   as
activated  carbon  adsorption  or chemical oxidation.  Therefore,
total suspended solids are not selected  for  limitation  in  the
bauxite refining subcategory.

TOXIC PRIORITY POLLUTANTS

The    frequency  of  occurrence  of  the  toxic  pollutants   in
the   wastewater samples taken is presented in Table  VI-1  (page
561).   These data  provide   the  basis for  the  categorization
of  specific pollutants, as discussed below.  Table VI-1 is based
on  the  raw wastewater  data  from  mud impoundment effluents at
plant  A  and plant  B  (see Section V).   All other  wastewaters
have  existing zero  discharge regulations  and  were   therefore
not   considered  here.    Treatment  plant   and  source   water
samples   were   not considered  in  this frequency count.

TOXIC POLLUTANTS NEVER DETECTED

The  toxic pollutants listed in Table VI-2 (page 565) were either
not  analyzed  or not detected in any wastewater    samples  from
this   subcategory;   therefore,  they  are  not   selected   for
consideration in establishing regulations:


We   did  not  analyze  for  selected pollutants  in  samples  of
raw wastewater from  this  subcategory.   These  pollutants   are
not  believed   to   be   present  based  on  the  Agency's  best
engineering  judgment  which  includes   consideration   of   raw
materials  and process operations.


TOXIC POLLUTANTS NEVER FOUND ABOVE THEIR ANALYTICAL
QUANTIFICATION LEVEL

The  toxic  pollutants listed in Table VI-3 (page 567) were never
found    above their  analytical quantification concentration  in
any   wastewater samples  from   this  subcategory;    therefore,
they   are    not  selected  for  consideration  in  establishing
                               556

-------
              BAUXITE REFINING SUBCATEGORY   SECT-VI
regulations,
TOXIC POLLUTANTS PRESENT BELOW CONCENTRATIONS ACHIEVABLE BY
TREATMENT

The pollutants listed below are not selected for consideration in
establishing  limitations  because  they  were  not  found in any
wastewater samples from  this  subcategory  above  concentrations
considered   achievable   by   existing  or  available  treatment
technologies.

 115. arsenic
 127. thallium

Arsenic was detected above its analytical quantification limit in
five of five samples from two plants.  These samples  were  below
the  0.34  mg/1 concentration considered achievable by treatment.
Therefore, arsenic is not selected for limitation.

Thallium was detected above its analytical  quantification  limit
in  one  of  five samples from two plants.  This sample was below
the 0.34 mg/1 concentration considered achievable  by  identified
treatment  technology.   Therefore,  thallium is not selected for
limitation.

TOXIC POLLUTANTS DETECTED IN A SMALL NUMBER OF SOURCES

The following pollutants were not selected for limitation because
they were detected in only a small number of sources:

 23. chloroform
 44. methylene chloride
 55. naphthalene
 60. 4,6-dinitro-o-cresol
 66. bis(2-ethylhexyl) phthalate
 68. di-n^butyl phthalate
 70. diethyl phthalate
 71. dimethyl phthalate
 77. acenaphthylene
 85. tetrachloroethylene

Although  these pollutants were not selected  for  consideration   in
establishing  nationwide limitations,  it  may be  appropriate, on a
case-by-case basis,  for  the  local  permitter  to   specify   effluent
limitations.

Chloroform  was  detected  above  its  treatable  limit  in  three  of  six
samples   from   two   plants  at  concentrations of  0.015,  0.026,  and
0.063 mg/1.  This pollutant  is not   attributable  to   any  source
within   the refinery.   It  also appears in the  source  water  and it
is commonly used  in  the  analytical   laboratories  as   a   solvent.
For these reasons chloroform is  not  considered  for limitation.

Methylene chloride was  found above its treatable concentration in
                                557

-------
               BAU&ITE REFINING SUBCATEGORY   SECT-VI


 three of four samples from two plants at concentrations of 0.020,
 0.051,  and  0.170  mg/1.    This pollutant is not attributable to
 specific materials or processes associated with bauxite refining.
 It is, however,  a common solvent used in analytical laboratories.
 Since  the  possibility  of  sample  contamination   is   likely,
 methylene chloride is not  selected for limitation.

 Naphthalene was  detected above its treatable concentration in one
 of  two  samples from one  plant, at a concentration of 0.02 mg/1.
 This pollutant is not attributable to bauxite refining operations
 or raw materials; it is also  present  only  slightly  above  the
 treatability  concentration.   For  these reasons, naphthalene is
 not considered for limitation.

 4,6-Dinitro-o-cresol   was   found   above    its    treatability
 concentration in one sample from one plant,  at a concentration of
 0.011  mg/1.   Because  this pollutant is not attributable to any
 specific  materials  or processes  in   the   bauxite   refining
 operation,  and it is present only slightly above the treatability
 concentration of  0.01 mg/1,  this pollutant is not selected for
 limitation.

 Bis(2-ethylhexyl)   phthalate  was  found  above   its   treatable
 concentration of  0.01 mg/1  in  five  of   six samples from two
 plants.    This  compound  is  a  plasticizer  commonly  used   in
 laboratory  and  field sampling  equipment and is not  used as a raw
 material  or   formed  as  a  by-product  in    this   subcategory.
 Therefore,    bis(2-ethylhexyl)   phthalate  is  not  selected  for
 limitation.

 Di-n-butyl phthalate was found  above its treatable  concentration
 of  0.01 mg/1  in  one of  six  samples from two  plants.   This
 compound is a plasticizer  commonly used in laboratory  and  field
 sampling equipment and is  not used as  a raw  material  or  formed as
 a    by-product   in   this   subcategory.   Therefore,   di-n-butyl
 phthalate  is  not  selected  for limitation.

 Diethyl  phthalate  was  found above  its  treatable concentration  of
 0.01 mg/1 in  one  of  two samples  from one plant.   This  compound is
 a  plasticizer  commonly used   in  laboratory  and field  sampling
 equipment and is  not  used as  a  raw material  or  formed   as   a   by-
 product  in this subcategory.  Therefore,  diethyl  phthalate  is  not
 selected for  limitation.

 Dimethyl phthalate was  found  above  its  treatable  concentration in
 one  of  two   samples   from  two plants  at a  concentration  of  1.5
 mg/1.  This pollutant  is not  attributable  to  specific  materials
 or   processes   associated   with  bauxite   refining.   The   high
 concentration  is probably due to   contamination   from   laboratory
 equipment.    Therefore,  dimethyl  phthalate  is  not selected  for
 limitation.

Acenaphthylene was  found   above   its  analytical  quantification
 limit  in  two of three  samples from two plants at concentrations
 of 0.018 and  0.086 mg/1.  This pollutant has  been  shown   to  be


                               558

-------
              BAUXITE  REFINING  SUBCATEGORY   SECT-VI


present  in the wastewater  from briquette quenching operations in
the primary aluminum subcategory.   The   two  sampled  plants  are
process, acenaphthylene is not selected for

Tetrachloroethylene was found above its treatability limit  in  one
samole from one plant, at a concentration of  0.012   mg/l.   Tnis
pollutant  is  nit attributable to any Process o^6!^
refininq  process;  it  is  present  only  slightly    above
"eatabilitj concentration of 0.01 mg/l and it is frequently used
in  the  laboratory,  where contamination could occur.  For these
reason!, tetrachloriethylene is not selected for limitation.

TOXIC POLLUTANTS  SELECTED FOR FURTHER CONSIDERATION FOR
LIMITATION

The     toxic  pollutants   listed  below   are    selected    for
further  consideration   in  establishing  limitations  for   this
subcategory.  The  selected pollutants are discussed individually
following  the list.
      2,4,6-tr ichlorophenol
      2-chlorophenol
      2,4-dichlorophenol
      2-nitrophenol
      4-nitrophenol
21.
24.
31,
57,
58
65.  phenol
       oncntationS ranging from 0.048 to 0.072            ^
 nf   those   samples  were  above  the  0.01   mg/l   concentration
 considered  achievable  by   identified   treatment    technology.
 Therefore,   2, 4, 6-tr ichlorophenol   is   selected    for   further
 consideration for limitation.
 2-Chlorophenol was  found  above  its  analytical quantification
 n£t IS two" of ?wo samples from one plant with concentrations of
 n nfis  and 0 720 mq/1.  Both of those samples were above  the  0.01
 mg/l5 Stability9 concentration.    Therefore    2-chlorophenol
 is selected for further consideration for limitation.

 2,4-Dichlorophenol  was found above its analytical  £££|Lf ication

                                    s? esvs
  limitation.

  2-Nitrophenol  was  found  above  its analytical quantification limit
  L one Sf SSree samples  from two Plants  at  a  conce ^ration  of
  0.067  mg/l.    That   sample  was above the 0.01 mg/l treatability
                                 559

-------
              BAUXITE REPINING SUBCATEGORY   SECT-VI
concentration.  Therefore, 2-nitrophenol is selected for
consideration for limitation.
further
4-Nitrophenol was found above its analytical quantification limit
in  three  of  four  samples  from two plants with concentrations
ranging from 0.017 to 0.310 mg/1.  Those three samples were above
the  0.01  rng/1  treatability   concentration.    Therefore,   4-
nitrophenol is selected for further consideration for limitation.

Phenol was found above its analytical quantification limit in six
of  six  samples from two plants with concentrations ranging from
0.034 to 0.750 mg/1.  All six of those  samples  were  above  the
0.01 _  mg/1 treatability concentration.  Also, phenols have  been
identified as constituents of bauxite ore.  Therefore, phenol  is
selected for further consideration for limitation.
                              560

-------
                    BAUXITE  REFINING  SUBCATEGORY
                                                                   SECT -  VI
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BAUXITE REFINING SUBCATEGORY
SECT - VI



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                 564

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             BAUXITE REFINING SUBCATEGORY   SECT-VI
                          TABLE VI-2

                TOXIC POLLUTANTS NEVER DETECTED

 2. acrolein*
 3« acrylonitrile*
 4. benzene*
 5. benzidene*
 7. chlorobenzene*
 8. 1,2,4-trichlorobenzene*
 9. hexachlorobenzene*
10. 1,2-dichloroethane*
11. 1,1,1-trichloroethane*
12. hexachloroethane*
13. 1,1-dichloroethane*
14. 1,1,2-trichloroethane*
15. 1,1,2,2-tetrachloroethane*
16. chloroethane*
17. bis (chloromethyl) ether (deleted)*
18. bis (2-ctiloroethyl) ether*
19. 2-chloroethyl vinyl  ether  (mixed)*
20. 2-chloronaphthalene*
22. parachlorometa   cresol
25. 1,2-dichlorobenzene*
26. 1,3-dichlorobenzene*
27. 1,4-dichlorobenzene*
28. 3,3'-dichlorobenzidine*
29. I,1-dichloroethylene*
30. 1,2-trans-dichloroethylene*
32. 1,2-dichloropropane*
33. 1,2-dichloropropylene (1,3-dichloropropene)*
35. 2,4-dinitrotoluene*
36. 2,6-dinitrotoluene*
37. 1,2-diphenylhydrazine*
38. ethylbenzene*
40. 4-chlorophenyl  phenyl ether*
41. 4-bromophenyl phenyl ether*
42. bis(2-chloroisopropyl) ether*
43. bis(2-choroethoxy)  methane*
45. methyl  chloride (chloromethane)*
46. methyl bromide (bromomethane)*
47. bromoform (tribromomethane)*
49. trichlorofluoromethane  (deleted)*
50. dichlorodifluoromethane (deleted)*
51. chlorodibromomethane*
52. hexachlorobutadiene*
53. hexachlorocyclopentadiene*
54. isophorone*
56. nitrobenzene*
59. 2,4-dinitrophenol
61. N-nitrosodimethylamine*
62. N-nitrosodiphenylamine*
63. N-nitrosodi-n-propylamine*
69. di-n-octyl  phthalate*
                              565

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              BAUXITE REFINING SUBCATEGORY   SECT-VI


                     TABLE VI-2  (Continued)

                 TOXIC POLLUTANTS NEVER DETECTED

 72. benzo(a)anthracene   (1,2-benzanthracene)*
 73. benzo  (a)pyrene  (3,4-benzopyrene)*
 74. 3,.4-benzofluoranthene*
 75. berizo(k)fluoranthane (11,12-benzofluoranthene)*
 76. chrysene*
 78. anthracene*
 79. benzo(ghi)perylene (1,11-benzoperylene)*
 81. phenanthrene*
 82. dibenzo (a,h)anthracene  (1,2,5,6-dibenzanthracene)*
 83. indeno (1,2,3-cd)pyrene  (w,e,-o-phenylenepyrene)*
 87. trichloroetnylene*
 88. vinyl chloride (chloroethylene)*
 89. aldrin*
 90. dieldrin*
 94. 4,4'-DDD(p,p'TDE)*
105. g-BHC-Delta*
113. toxaphene*
116. asbestos
117. beryllium*
118. cadmium*
119. chromium (Total)*
120. copper*
122. lead*
123. mercury*
124. nickel*
128. zinc*
129. 2,3,7,8-tetrachlorodibenzo-p-dioxin (TCDD)

* Pollutants not analyzed for.
                               566

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            BAUXITE REPINING SUBCATEGORY   SECT-VI
                         TABLE VI-3

         PRIORITY POLLUTANTS  NEVER FOUND ABOVE  THEIR
               ANALYTICAL QUANTIFICATION LEVEL
   1.
   6.
  34.
  39.
  48.
  64.
  67.
  80.
  84.
  86.
  91.
  92.
  93.
  95.
  96.
  97.
  98.
  99.
100.
101.
102.
103.
104.
106.
107.
108.
109.
110.
111.
112.
114.
121.
125.
126.
 acenaphthene
 carbon  tetrachloride  (tetrachloromethane)
 2,4-dimethylphenol
 fluoranthene
 dichlorobromomethane
 pentachlorophenol
 butyl benzyl phthalate
 fluorene
 pyrene
 toluene
 chlordane  (technical mixture and metabolites)
 4,4'-DDT
 4,4'-DDE(p,p'DDX)
 a-endosulfan-Alpha
 b-endosulfan-Beta
 endosulfan sulfate
 endrin
 endrin aldehyde
 heptachlor
 heptachlor epoxide
 alpha-BHC
 beta-BHC
 r-BHC (lindane)-Gamma
 PCB-1242 (Arochlor 1242)
 PCB-1254 (Arochlor 1254)
 PCB-1221 (Arochlor 1221)
 PCB-1232 (Arochlor 1232)
 PCB-1248 (Arochlor 1248)
 PCB-1260 (Arochlor 1260)
PCB-1016 (Arochlor 1016)
antimony
cyanide (Total)
selenium
silver
                            567

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BAUXITE REFINING SUBCATEGORY   SECT-VI
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                  568

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               BAUXITE REFINING SUBCATEGORY   SECT-VII




                           SECTION VII

               CONTROL AND TREATMENT TECHNOLOGIES
The  preceding sections of this supplement discussed the sources,
flows/ and characteristics of the wastewaters  generated  in  the
bauxite   refining  subcategory.   This  section  summarizes  the
description of these  wastewaters  and  indicates  the  level  of
treatment which is currently practiced for each waste stream.

CURRENT CONTROL AND TREATMENT PRACTICES

Control  and  treatment  technologies are discussed in general in
Section VII of  the  General  Development  Document.   The  basic
principles  . of  these  technologies  and  the  applicability  to
wastewater  similar  to  that  found  in  this  subcategory   are
presented  there.  This section presents a summary of the control
and treatment technologies that are currently applied to each  of
the  sources  generating  wastewater  in  this,  subcategory.   As
discussed in Section V, wastewater associated  with  the  bauxite
refining   subcategory   is  characterized  by  the  presence  of
treatable concentrations of phenolic compounds and high pH.  This
analysis is supported by  the  raw  (untreated)  wastewater  data
presented  for  specific  sources  in  Section  V.   According to
promulgated BPT limitations (40 CFR Part  421,  Subpart  A),  the
only allowable discharge of wastewater pollutants for the bauxite
refining   subcategory  is  the net precipitation discharge  from
the   red   mud  impoundment.    The  other  three   subdivisions
(digester   condensate,   barometric   condenser  effluent,   and
carbonation plant effluent) are all restricted to zero  discharge
of  wastewater  pollutants under the promulgated BPT  regulation.
Three  plants  in this subcategory  currently  discharge  treated
water  from  the  mud  impoundment area.   One  option  has  been
selected for consideration for BPT, BAT, NSPS,  and  pretreatment
based on this waste stream.

MUD IMPOUNDMENT EFFLUENT

Red   mud  is  the  major  waste  stream  from  bauxite  refining
operations.  It contains the impurities from the bauxite  ore  as
well  as by-products formed during the refining process.  Red mud
is deposited in large ponds where insoluble solids, including the
oxides of metallic elements, settle out of suspension.   Rainfall
from  the  plant  site  is  often  routed to the mud impoundment.
Water from the impoundment can be recycled to the plant  directly
from  the mud lake or it can be decanted to a separate clear lake
before recycle.

Three plants currently discharge water from the mud  impoundment.
At  one  plant,  water  is discharged after pH adjustment without
recycle to the process.  At another plant, a portion of the water
                               569

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               BAUXITE REFINING SUBCATEGORY   SECT-VII
which is recycled to the plant from a clear  lake  is  discharged
without  treatment.  The third plant discharges excess stormwater
from closed mud lakes after pH adjustment.   The  remaining  five
plants  in  this  subcategory currently achieve zero discharge by
permanent lagoon impoundment and partial recycle.   However,  one
of  these plants is considering a process technology change which
would result in a mud impoundment discharge.

CONTROL AND TREATMENT OPTIONS

Although  the existing limitations are not  being  modified,  the
Agency  examined  one control and treatment alternative  that  is
applicable  to   the  bauxite  refining  subcategory to  generate
the guidance limitations.   The  option selected  for  evaluation
represents  an  end-of-pipe  treatment technology.
                                                               of
                                                               of
                                                              net
                                                               pH
                                                              the
OPTION E

Option  E  for the bauxite refining  subcategory   consisted
all  control  requirements of the existing BPT (no  discharge
process   wastewater    pollutants,    and   discharge   of
precipitation  from  process  wastewater  impoundments)  plus
adjustment  and  activated carbon adsorption treatment   of
mud  impoundment  effluent.  Activated  carbon adsorption is used
to  remove  organic  compounds,  including  phenolics,  from  the
effluent wastewater.   Adjustment of pH is  required  to   ensure
consistent   removal   performance   by adsorption  and  to  meet
discharge quality standards.

The  Agency also considered the use of pH adjustment and chemical
oxidation  to  remove  phenolic  compounds  from   the   effluent
wastewater.   Adjustment  of  pH is required to ensure consistent
discharge quality  standards.   Hydrogen  peroxide  is  suggested
for  the oxidation of phenols,   but  other  chemicals,  such  as
chlorine dioxide and ozone, may perform satisfactorily.
                              570

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           BAUXITE REFINING SUBCATEGORY   SECT-VIII




                          SECTION VIII

            COSTS OP WASTEWATER TREATMENT AND CONTROL
The  Agency  is  not  revising  the  promulgated  regulation  for
discharges from bauxite refining.    Therefore there are no costs
associated with this rulemaking.    This  section  describes  the
method   used  to develop the costs associated with the  guidance
control  and  treatment technologies of  Option E   discussed  in
Section VII for wastewaters from bauxite refining plants.  Plant-
by-plant  compliance  costs  for  this  option   were  developed.
Compliance   costs  for  chemical oxideition were also  estimated.
The  energy  requirements of the considered  option  as  well  as
solid  waste and air pollution aspects are  also  discussed.  The
General    Development    Document    provides background on  the
capital  and annual  costs  for  the  technology discussed herein
and the methodology used to develop compliance costs.

TREATMENT OPTIONS COSTED FOR EXISTING SOURCES

As  discussed  in  Section  VII,  one  treatment  option has been
considered for existing bauxite refining plants.  This option  is
summarized  below  and is schematically presented in  Figure  X-l
(page 582).

OPTION E

Option E consists of the BPT requirements with additional control
of  the mud impoundment discharges by pH adjustment and activated
carbon adsorption.  The Agency also prepared capital  and  annual
costs  for  pH  adjustment  and  chemical  oxidation  of  the mud
impoundment effluent at one median plant.  The  calculated  costs
were much higher in relation to the costs for activated carbon at
the  same plant, therefore, no further consideration was given to
this, technology.

COST METHODOLOGY

Plant-by-plant  compliance costs have  been estimated  for   this
subcategory.  The   costs for the option in this subcategory  are
presented in Table VIII-1 (page 573).  The major assumptions specific
bauxite refining subcategory are discussed briefly below.

(1) The Option E  treatment  system  consists  of  pH  adjustment
followed by carbon adsorption.  The  flows  were  determined from
information  provided  in  the  dcp  for  red   mud   impoundment
discharge  flow  only.    The  influent concentrations for phenol
and  2-chlorophenol  were  determined  from  averages   of  field
sampling data from two plants. These data are found in Table  V-5
(page 549).

(2) Costs for pH adjustment were based on reduction  of  pH  from
                               571

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           BAUXITE REFINING SUBCATEGORY   SECT-VIII
11.5 to 9 using sulfuric acid.

(3)  The  carbon  exhaustion  rate was determined from adsorption
isotherms for phenol and 2-chlorophenol, influent  concentrations
from  the  sampling  data,  and an effluent concentration in both
cases of 0.010 mg/1.   Using this procedure and an excess  of  50
percent  to  account  for  other  adsorbable organics,  a  carbon
exhaustion rate of 2.321 lbs/1000 gallons was determined.

(4) Plants 1076 and 1141 have pH adjustment equipment  in  place;
capital  cost  estimates  are included for all other equipment at
the three discharging plants and the one existing zero discharger
who is considering a discharge.

NONWATER QUALITY ASPECTS

Nonwater  quality  impacts  specific  to  the  bauxite   refining
subcategory,   including  energy  requirements,  solid waste  and
air pollution are discussed below.

ENERGY REQUIREMENTS

Energy   requirements  for  Option  E are estimated at 11,500,000
kwh/yr.   This  represents  less  than  3 percent  of  the  total
energy  usage of the four plants.  It is therefore concluded that
the  energy requirements of the treatment option considered  will
not   have  a   significant   impact   on   total  plant   energy
consumption.

SOLID WASTE

No  significant  amounts  of  solid  wastes  are generated by the
technologies  considered  for  this  regulation  in  the  bauxite
refining  subcategory.  Activated carbon is thermally regenerated
either on-site or off-site, and in neither case  are  appreciable
quantities of solid waste generated.

AIR POLLUTION

There  is no reason to believe that any substantial air pollution
problems will result  from  implementation  of  activated  carbon
treatment  and  pH  adjustment.   Thermal  regeneration  of spent
carbon may release trace  quantities  of  pollutants,  but  these
should  be  readily  oxidized at the temperatures under which the
carbon is regenerated.
                               572

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      BAUXITE REFINING SUBCATEGORY   SECT-VIII
                     Table VIII-1

COST OF COMPLIANCE FOR THE BAUXITE REFINING SUBCATEGORY
                  DIRECT DISCHARGERS*

                       (March, 1982 Dollars)
   Option

     E
      Proposal

Total Required
 Capital Cost

  7,600,000
   Total
Annual Cost

 2,980,000
*Includes one plant currently practicing zero discharge of
 process wastewater.
                          573

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BAUXITE REFINING SUBCATEGORY   SECT-VIII
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                   574

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              BAUXITE REFINING SUBCATEGORY   SECT-IX



                           SECTION IX

         BEST PRACTICABLE TECHNOLOGY CURRENTLY AVAILABLE
BPT  limitations  for  the   bauxite   refining subcategory  were
promulgated on  April  8,   1974 as Sufopart A of 40 CFR Part 421.
EPA  is  not amending these BPT limitations which are  reproduced
below.

The  following  limitations  establish the quantity or quality of
pollutants or pollutant properties which may be discharged  by  a
point  source  after  application of the best practicable control
technology  currently available:  There shall be   no   discharge
of process wastewater pollutants to navigable waters.

During  any  calendar  month,  there  may  be discharged from the
overflow of a process wastewater impoundment either a  volume  of
wastewater  equal to the difference between the precipitation for
that month that falls within the impoundment and the  evaporation
within  the  impoundment for that month, or, if greater, a volume
of process wastewater equal to the difference  between  the  mean
precipitation  for  that  month that falls within the impoundment
and the mean evaporation for that month  as  established  by  the
National   Climatic  Center,  National  Oceanic  and  Atmospheric
Administration, for the area in which such impoundment is located
(or  as  otherwise  determined  if  no  monthly  data  have  been
established by the National Climatic Center).

The  data gathered since the original promulgation do not warrant
any  adjustment  in  the  BPT  requirements.  Minor amendments to
the  regulatory  language  are  being  promulgated  to    clarify
references    to    fundamentally    different    factors   (FDF)
considerations      under    40    CFR     Part     -125       and
references    to pretreatment  standards  under 40 CFR Part  128.
As a result,  the bauxite refining  subcategory  will  not  incur
any   incremental capital or annual costs to comply with the  BPT
limitations.
                               575

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BAUXITE REPINING SUBCATEGORY   SECT-IX
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                576

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              BAUXITE REFINING SUBCATEGORY   SECT-X



                            SECTION X

        BEST AVAILABLE TECHNOLOGY ECONOMICALLY ACHIEVABLE
These  effluent  limitations are based on the  best  control  and
treatment  technology  used  by   a  specific    point     source
within   the   industrial   category   or  subcategory,   or   by
another    industry   where   it    is    readily   transferable.
Emphasis    is   placed   on   additional   treatment  techniques
applied at the end of the treatment systems  currently used,   as
well    as   reduction   of   the   amount  of  water  used   and
discharged,,   process   control,   and    treatment    technology
optimization.

The  factors  considered  in  assessing best available technology
economically achievable (BAT) include the age  of  equipment  and
facilities  involved, the process used, process changes, nonwater
quality environmental impacts  (including  energy  requirements),
and   the  costs  of  application  of  such  technology  (Section
304(b)(2)(B)  of  the  Clean  Water  Act).   At  a  minimum,  BAT
represents  the best available technology economically achievable
at  plants  of  various  ages,   sizes,   processes,   or   other
characteristics.    Where  the  Agency  has  found  the  existing
performance to be uniformly inadequate, BAT  may  be  transferred
from  a  different  subcategory  or  category.   BAT  may include
feasible process changes or internal controls, even when  not  in
common industry practice.

The  required  assessment  of  BAT  considers costs, but does not
require a balancing of costs against effluent reduction  benefits
However,  in assessing BAT,   the  Agency  has  given substantial
weight   to   the  economic  achievability  of  the technology.

TECHNICAL APPROACH TO BAT

In pursuing this second round of effluent limitations, the Agency
reviewed a wide range of technology  options  and  evaluated  the
available  possibilities  to  ensure  that the most effective and
beneficial technologies were  used  as  the  basis  of  BAT.   To
accomplish  this,  the  Agency  elected to examine one technology
option which could be applied to the bauxite refining subcategory
as an alternative for the basis of BAT effluent limitations.  The
treatment technology considered for BAT is summarized below:


Option E (Figure X-l page 582):

o   Zero discharge of process wastewater pollutants
o   Discharge of net precipitation from process wastewater
    impoundments
                               577

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              BAUXITE REFINING SUBCATEGORY   SECT-X
    pH adjustment
    Activated carbon adsorption
OPTION E

Option E. consists of the existing BPT requirements (no  discharge
of  process wastewater pollutants, discharge of net precipitation
from a process wastewater impoundment), with  pH  adjustment  and
activated  carbon  adsorption  treatment of the net precipitation
discharge.  Activated carbon technology is used to  remove  toxic
organic   compounds,   including  phenolics,  from  the  effluent
wastewater.  Adjustment of pH is required  to  ensure  consistent
removal  performance  by adsorption and to meet discharge quality
standards.

INDUSTRY COST AND POLLUTANT REMOVAL ESTIMATES

As one means of evaluating the technology option,  EPA  developed
estimates  of  the pollutant removal estimates and the associated
compliance costs.  The methodologies are described below.

POLLUTANT REMOVAL ESTIMATES

Sampling   data collected  during  the  field  sampling   program
were  used   to characterize  the  pollutant  concentrations   in
the waste stream considered for regulation.  This information was
used   with   the wastewater  discharge  rates   measured  during
sampling  or derived from each dcp to estimate the mass of  toxic
pollutants   generated  by  each plant in  the  bauxite  refining
subcategory.  The  mass of pollutant discharged was estimated  by
multiplying  the achievable  concentration  values attainable  by
the   option  (mg/1)  by  the  estimated  volume  of   wastewater
discharged  by  each  plant  in the  subcategory.   The  mass  of
pollutant removed,  referred  to  as the  benefit,  is simply the
difference  between the estimated mass of pollutant generated  by
each  plant  and  the   mass   of   pollutant  discharged   after
application  of  the treatment  option.   The  total  subcategory
removal  was  then  estimated by summing  the   individual  plant
removal   estimates   for   each   pollutant.     The   pollutant
removal  estimates  for  the  bauxite  refining  subcategory  are
presented in Table X-l (page 580).

COMPLIANCE COSTS

Based  on  information  collected  after  proposal,   the  Agency
believes  that  no  further  revisions  to  the  promulgated  BAT
limitations  are necessary.   As a result,  the bauxite  refining
subcategory  will  not  incur any incremental capital  or  annual
costs  to  comply  with  the  BAT  limitations.     However,  EPA
calculated    compliance   costs  •for   the   bauxite   refining
subcategory by developing a wastewater  treatment  system  design
and cost estimation model that estimates capital and annual costs
for   the   treatment  option  being   considered  for  guidance.
This   model  was  applied  to each plant's  flow  arid  pollutant
                               578

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              BAUXITE REFINING SUBCATEGORY   SECT-X
characteristics,   and  the  calculated capital and annual  costs
were summed to arrive at total subcategory costs.   These  costs,
which   are   presented  in Table X-2 (page 583),   were used  in
EPA's economic impact analysis.

BAT OPTION SELECTION

EPA   promulgated   BAT  limitations  for  the  bauxite  refining
subcategory on April 8, 1974 as Subpart A of  40  CFR  Part  421.
These  limitations  allow  no  discharge  of  process  wastewater
pollutants to navigable waters.  A discharge is allowed from  the
overflow of a process wastewater impoundment in a volume equal to
the  net precipitation that falls within the impoundment.  EPA is
not  promulgating  any modification to these limitations at  this
time.  At  proposal,  EPA  was considering the  establishment  of
effluent   limitations     based    on    pH    adjustment    and
activated    carbon  adsorption  treatment  of   toxic    organic
pollutants  in  the  mud impoundment  overflow.    This  revision
was  in keeping with the emphasis of the Clean Water Act of  1977
on toxic pollutants.

Implementation  of  this  organics  control  option   would  have
removed  annually  an  estimated 4,835 kg of priority  pollutants
from the raw discharge.   Estimated capital  cost  for  achieving
this   option  would   have been $7.60  million,  with  estimated
annualized costs of $2.98 million.

Activated  carbon was being considered because of   its   ability
to remove  toxic  organics  to very low concentrations.  Although
no  plants  in  the  nonferrous  metals  manufacturing   category
have  installed   this   technology   for    organics    removal,
it    is  demonstrated  in  the  iron  and  steel   manufacturing
category.    EPA  believes  that  the  influent   characteristics
are  similar with respect to organics for both  categories,   and
that,  if  proper design  procedures  are  used, similar removals
will  be  achieved.   Activated  carbon  will  remove  adsorbable
organics   to  essentially nondetectable  levels  if   sufficient
carbon and contact time are provided.   These  design  parameters
have   been   carefully  and conservatively  selected by EPA  for
this subcategory.   Therefore,  based on these considerations and
the  performance  data from  iron and   steel   manufacturing   a
level   of  0.010  mg/1 for  phenol,  2-chlorophenol,  and  total
phenols  (4-AAP)   can  be  achieved.    The  Agency    solicited
comments  on  the  costs  and  performance  of activated  carbon,
and  the  applicability  of  these   effluent limitations to  the
bauxite refining subcategory.

Commenters  on the proposal provided recently collected data from
their  red mud lakes showing levels below the limit of  detection
for all phenolic compounds except phenol.  The new data submitted
indicates that EPA may have overestimated the amounts of  phenols
in  the  net precipitation discharge from bauxite red mud  lakes.
Based on these data,  EPA has  decided not to promulgate Option  E
(pH  adjustment,  activated carbon adsorption) as the  technology
basis  of BAT.   EPA has determined that the presence of  phenols
                               579

-------
               BAUXITE REFINING SUBCATEGORY    SECT-X
 may be  site-specific  and  not  common  to  all  bauxite manufacturers.
 Furthermore,    EPA's    analysis   showed  no  harmful   effects  on
 aquatic life,   and  only some  taste and  odor  effects.  EPA  is  not
 modifying   the  existing BAT regulation  for  the   bauxite  refining
 subcategory.    However,  EPA  is  publishing  limitations,  shown  at
 the  end   of   this  section,    as   guidance     for    permitting
 authorities to  deal  with   any site-specific   high  levels  of
 phenolic compounds.

 REGULATED  POLLUTANT PARAMETERS

 The raw wastewater  concentrations from  individual operations  and
 the subcategory  as  a  whole were  examined  to select   certain
 pollutants and  pollutant   parameters  for  limitation.   This
 examination  and  evaluation,    presented  in  Section   VI,
 concluded    that    six  pollutants  and    pollutant   parameters
 are present  in  bauxite refining wastewaters at  concentrations
 that  can   be   reduced  by identified treatment  technologies.

 The    high  cost    associated  with   analysis  for   priority
 organic pollutants   had  prompted EPA to  consider an  alternative
 method  for regulating and monitoring pollutant   discharges   from
 the nonferrous  metals  manufacturing  category.    Rather  than
 developing specific  effluent limitations and standards for  each
 of  the organics  pollutant found in treatable concentrations  in
 the raw wastewater from  a given subcategory,    the  Agency   was
 considering  effluent  limitations  only   for   those  pollutants
 generated   in   the  greatest quantities  as shown  by the  pollutant
 removal estimate  analysis.  On this  basis,   the   pollutants
 recommended for specific  limitation at  proposal  are listed below:

 24. 2-chlorophenol
 65. phenol

 By   recommending  limitations   and    standards   for     certain
 priority organic  pollutants,    dischargers would attain the same
 degree   of  control   over  priority organic  pollutants  as   they
 would    have    been required  to  .achieve   had   all the  priority
 organic  pollutants   been  directly  limited.   This  approach  is
 technically  justified  because  the design of   activated  carbon
 columns  must consider  the presence of  other  organic   compounds
 which   will  be  removed  from  the wastewater.     Even   though
 the   removal   of  different  phenolic compounds will  occur  at
 different   rates,  treatment of  the  above listed  organics   to
 the   concentration   values  attainable by  the  option  will  be
 accompanied  by   a reduction in  concentration of the  unregulated
 organics.    One  nonconventional   pollutant   parameter,   total
 phenols    (4-AAP),  was being considered for limitation to ensure
 adequate   removal of  phenolics  other   than   2-chlorophenol  and
phenol.    No priority metal pollutants were selected for specific
 limitation  in this subcategory.

The  following  priority pollutants  were not  being   considered
 for  specific   limitation at .proposal  on  the  basis  that  they
would   be   effectively   controlled   by    the     limitations
                               580

-------
              BAUXITE REFINING SUBCATEGORY   SECT-X
recommended for
AAP) :
2-chlorophenol, phenol, and total phenols   (4-
 21. 2,4,6-trichlorophenol
 31. 2,4-dichlorophenol
 57. 2-nitrophenol
 58. 4-nitrophenol

The  conventional  pollutant  parameter  pH may be limited by the
best conventional technology (BCT) effluent limitations.

EFFLUENT LIMITATIONS

The concentrations achievable by application of pH adjustment and
activated carbon are discussed in  Section  VII  of  the  General
Development Document. The    recommended     effluent limitations
for    mud   impoundment  effluent   are   shown   below.   These
effluent limitations are presented as guidance for state or local
pollution   control  agencies  for   case-by-case   control    of
phenolics.
RECOMMENDED   GUIDANCE   FOR  BAT  EFFLUENT  LIMITATIONS
FOR  THE  BAUXITE REFINING SUBCATEGORY
Mud Impoundment Effluent
Pollutant or
Pollutant Property
                      Maximum for
                    Any One Day (mg/1)
2,4,6-trichlorophenol
2-Chlorophenol
2,4-dichlorophenol
4-nitrophenol
Phenol
Total Phenols (4-AAP)
                        0.010
                        0.010
                        0.010
                        0.010
                        0.010
                        0.010
                               581

-------
               BAUXITE REFINING  SUBCATEGORY   SECT-X
                            TABLE X-l

                   POLLUTANT REMOVAL ESTIMATES
                        BAUXITE REFINING
                   (Direct Dischargers* - kg/yr)
Pollutant
2-chlorophenol
phenol
Total Raw
                  Current
3,125.51
1,868.95
Total toxic organics   4,994.45
Discharged
 3,125.51
 1,868.95

 4,994.45
Removed
   0
   0
                 Option E
2-chlorophenol
phenol
Total toxic organics
                  79.53
                  79.53

                 159.06
                3,045.98
                1,789.42

                4,835.40
* Includes one small plant currently practicing zero discharge of
process wastewater.
                               582

-------
              BAUXITE REFINING SUBCATEGORY   SECT-X



                               Table X-2

     COST OF COMPLIANCE FOR THE BAUXITE REFINING SUBCATEGORY

                       Direct Dischargers*
          Proposal
           Option

             E
 Capital Cost
(1982 Dollars)

 7,600,000
  Annual Cost
(1982 Dollars)

 2,980,000
*Includes one small plant currently practicing zero discharge  of
process wastewater.
                               583

-------
BAUXITE REFINING SUBCATEGORY
SECT  - X
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                   584

-------
              BAUXITE REFINING SUBCATEGORY   SECT-XI



                           SECTION XI

                NEW SOURCE PERFORMANCE STANDARDS
The  basis  for  new  source  performance  standards (NSPS) under
Section 306  of  the  Act  is  the  best  available  demonstrated
technology  (BDT).  New plants have the opportunity to design the
best and  most  efficient  production  processes  and  wastewater
treatment   technologies  without  facing  the  added  costs  and
restrictions  encountered  in  retrofitting  an  existing  plant.
Therefore,   Congress   directed   EPA   to   consider  the  best
demonstrated process changes, in-plant controls, and  end-of-pipe
treatment  technologies  which  reduce  pollution  to the maximum
extent feasible.

This  section-  describes  the  technologies  for   treatment   of
wastewater   from   new  sources  and  presents  the  performance
standards  recommended  as guidance for  NSPS  in   the   bauxite
refining subcategory, based on the selected treatment technology.

TECHNICAL APPROACH TO NSPS

EPA  promulgated new source performance standards for the bauxite
refining subcategory on April 8 1974.  The technology  basis  for
this   promulgation  was  identical to BAT.   EPA is promulgating
only  minor technical amendments to the  promulgated  regulation.
It  is also  recommending as guidance the  limitations  described
in  the  previous section  for  BAT,   i.e.,  pH  adjustment  and
activated   carbon  adsorption  of  mud   impoundment   overflow.
This   result  is  a consequence of careful review by the  Agency
of  a   wide   range  of technology  options   for   new   source
treatment  systems  which  is discussed in Section  XI   of   the
General  Development  Document.  Additionally,  there was nothing
found  to indicate that the wastewater flows and  characteristics
of  new  plants would  not  be similar  to  those  from  existing
plants,  since the processes used by new sources are not expected
to  differ  from  those  used  at existing sources.

The   treatment  technology  considered  for  the  NSPS  guidance
option is identical to the treatment  technology  considered  for
the  BAT guidance option.  This option is:

OPTION E

 o Zero discharge of process wastewater pollutant
 o Discharge  of net precipitation from process  wastewater
   impoundments
 o pH adjustment
 o Activated carbon adsorption
                               585

-------
               BAUXITE  REFINING  SUBCATEGORY    SECT-XI
 NSPS  OPTION  SELECTION
As   discussed   earlier,  with   the   exception  of minor technica.
amendments,  the Agency  is  not modifying  the existing  promulgate!
regulation   for  the bauxite refining subcategory.  The Agency is
recommending  the standards presented at  the end of this  sectior
as   guidance  for permitting authorities  to deal with  any  site-
specific high  levels of phenolic compounds.


REGULATED POLLUTANT PARAMETERS

The  Agency has  no reason to believe  that  the pollutants that will
be   found  in   treatable   concentrations  in processes within new
sources  will   be any  different  than   with  existing  sources.
Accordingly,    pollutants   and   pollutant   parameters   being
recommended    for  limitation  as   guidance  under    NSPS,   in
accordance with the rationale of Sections VI and X, are identical
to   those    being  recommended  for  BAT.     The   conventional
pollutant    parameter  pH  is also being  recommended as  guidance
for  limitation.   For  NSPS,  the  Agency  is   recommending  as
guidance pH  limitations   for mud impoundment effluent within the
range of 7.5   to   10.0  at  all  times.

NEW  SOURCE PERFORMANCE STANDARDS

The    modified   performance  standards  being  recommended   as
guidance  based on pH adjustment and activated carbon  adsorption
technology are  listed below.
RECOMMENDED
SUBCATEGORY
GUIDANCE   FOR  NSPS  FOR  THE   BAUXITE
REFINING
Mud Impoundment Effluent
Pollutant or
Pollutant Property
                         Maximum for
                      Any One Day (mg/1)
2,4,6-trichlorophenol
2-Chlorophenol
2,4-dichlorophenol
4-nitrophenol
Phenol
Total Phenols (4-AAP)
                           0.010
                           0.010
                           0.010
                           0.010
                           0.010
                           0.010
                               586

-------
               BAUXITE REFINING SUBCATEGORY   SECT-XII



                           SECTION XII

                     PRETREATMENT STANDARDS
EPA   is  not promulgating pretreatment  standards  for  existing
sources  at  this  time because there are currently  no  indirect
discharging facilities in this subcategory.

EPA  promulgated  PSNS  for  the  bauxite refining subcategory on
April 8,  1974 as Subpart A of 40 CFR Part  421.   The  following
limitations  establish  the  quantity or quality of pollutants or
pollutant properties which may be discharged by  a  new  indirect
discharger:  There  shall  be  no discharge of process wastewater
pollutants to navigable waters.

During any calendar month,  there  may  be  discharged  from  the
overflow  of  a process wastewater impoundment either a volume of
wastewater equal to the difference between the precipitation  for
that  month that falls within the impoundment and the evaporation
within the impoundment for that month, or, if greater,  a  volume
of  process  wastewater  equal to the difference between the mean
precipitation for that month that falls  within  the  impoundment
and  the  mean  evaporation  for that month as established by the
National  Climatic  Center,  National  Oceanic  and   Atmospheric
Administration, for the area in which such impoundment is located
(or  as  otherwise  determined  if  no  monthly  data  have  been
established by the National Climatic Center).

EPA  is not promulgating any  modifications  to  PSNS  since   it
is unlikely  that  any  new  bauxite  sources will be constructed
as indirect dischargers.
                                587

-------
BAUXITE REFINING SUBCATEGORY   SECT-XII
THIS PAGE INTENTIONALLY LEFT BLANK
                588

-------
           BAUXITE REFINING SUBCATEGORY   SECT-XIII




                          SECTION XIII

         BEST CONVENTIONAL POLLUTANT CONTROL TECHNOLOGY
EPA    is   not   promulgating  best   conventional     pollutant
control  technology  (BCT) limitations for the  bauxite  refining
subcategory at this time.
                                589

-------
BAUXITE REPINING SUBCATEGORY   SECT-XIII
    THIS  PAGE INTENTIONALLY LEFT BLANK
                   590

-------
NONFERROUS METALS MANUFACTURING POINT SOURCE CATEGORY
           DEVELOPMENT DOCUMENT SUPPLEMENT
                       for the
        Primary Aluminum Smelting Subcategory
                  William K. Reilly
                    Administrator
                   Rebecca Hanmer
      Acting Assistant Administrator for Water
              Martha Prothro, Director
      Office of Water Regulations and Standards
            Thomas P. O'Farrell, Director
            Industrial Technology Division
             Ernst P. Hall, P.E., Chief
               Metals Industry Branch
                         and
              Technical Project Officer
                     May  1989
        U.S.  Environmental  Protection Agency
                   Office of Water
      Office  of Water  Regulations and Standards
            Industrial  Technology Division
              Washington, D. C.  20460
                          591

-------
592

-------
                 PRIMARY ALUMINUM SUBCATEGORY
                        TABLE OF CONTENTS
Section

I

II

III
IV
V
SUMMARY AND CONCLUSIONS

RECOMMENDATIONS

INDUSTRY PROFILE

Description of Primary Aluminum Production
Raw Materials
Electrolytic Aluminum Production
Reduction Cells
Aluminum Fluxing and Degassing
Casting
Anode Paste Plant
Anode Bake Plant
Cathode Reprocessing
Procecess Wastewater Sources
Other Wastewater Sources
Age, Production, and Process Profile

SUBCATEGORIZATION

Factors Considered in Subdividing the
  Primary Aluminum Subcategory
Other Factors
Type of Anode
Plant Size
Plant Age
Product
Production Normalizing Parameters
Anode and Cathode Paste Plant Wet Air
  Pollution Control
Cathode Reprocessing
Potlihe, Potline SO2, and Potroom Wet Air
Pollution Control

WATER USE AND WASTEWATER CHARACTERISTICS

Wastewater Sources, Discharge Rates, and
Characteristics
Anode and Cathode Paste Plant Wet Air
  Pollution Control
Anode Bake Plant Wet Air Pollution Control
Anode and Briquette Contact Cooling
Cathode Reprocessing
Potline Wet Air Pollution Control
603

607

627

627
627
627
627
630
632
633
635
635
636
636
637

643

643

643
643
644
644
644
644
645

641
645
649

650

652

653
653
653
654
                               593

-------
                 •PRIMARY ALUMINUM  SUBCATEGORY
                  TABLE OF CONTENTS  (Continued)
 Section

 V
 (Cont'd)
VI
VII
 Potline SO2  Wet  Air  Pollution  Control             654
 Potroom Wet  Air  Pollution  Control                 654
 Degassing  Wet  Air  Pollution  Control               654
 Pot  Repair And Pot Soaking                       655
 Casting Contact  Cooling Water                     655
 Pilot  Scale  Wastewater Treatment Study            656
 PAH  Treatment                                     656
 Cyanide Treatment                                 657

 SELECTION  OP POLLUTANT PARAMETERS                 725

 Conventional And Nonconventional Pollutant        725
  Parameters
 Conventional And Nonconventional Pollutants       726
  Parameters Selected
 Toxic  Pollutants                                 726
 Toxic  Pollutants Never Detected                   727
 Toxic  Pollutants Never Found Above Their          727
  Analytical Quantification Level
 Toxic  Pollutants Present Below Concentrations     727
  Achievable By  Treatment
 Toxic  Pollutants Detected  In a Small Number       727
  Of Sources
 Toxic  Pollutants Selected  For Further             730
  Consideration  For Limitations

 CONTROL AND  TREATMENT TECHNOLOGIES                743

 Technical  Basis  Of BPT                            743
 Current Control  And Treatment Practices           743
 Anode And  Cathode Paste Wet Air Pollution         744
  Control
 Anode Bake Plant Wet Air Pollution Control        744
 Anode And  Briquette Contact Cooling               745
 Cathode Reprocessing                              745
 Potline And  Potroom Wet Air Pollution Control     745
 Pot Repair And Pot Soaking                        747
 Degassing Wet Air Pollution Control               747
 Casting Contact  Cooling                           748
 Control And  Treatment Options                     748
 Option A                                          749
Option B                                          749
Option C                                          749
Option E                                          750
Control And Treatment Options Rejected            750
Fluoride Treatment Effectiveness Analysis         750
Treatment Effectiveness Analysis For Potline      750
  Srubbers And Cathode Reprocessing Wastewate rs
                               594

-------
                 PRIMARY ALUMINUM SUBCATEGORY
                  TABLE OP CONTENTS (Continued)
Section
VIII
                                             Page
IX

X
COSTS, ENERGY, AND NONWATER QUALITY ASPECTS

Levels Of Treatment Considered
Option A
Option B
Option C
Option E
Cost Methodology
Nonwater Quality Aspects
Energy Requirements
Solid Waste
Air Pollution

BEST PRACTICABLE TECHNOLOGY CURRENTLY AVAILABLE

BEST AVAILABLE TECHNOLOGY ECONOMICALLY
ACHIEVABLE

Technical Approach To BAT
Option A
Option B
Recycle of Anode and Casting Contact Cooling
  Water Through Cooling Towers
Recycle of Water Used in Wet Air Pollution
  Control
Option C
Option E
Industry Cost And Pollutant Removal Estimates
Pollutant Removal Eestimate
Compliance Costs
BAT Option Selection
Final Amendments To The Regulation
Treatment Performance
Wastewater Discharge Rates
Anode And Cathode Paste Plant Wet Air Pollution
  Control Wastewater
Anode Bake Plant Wet Air Pollution Control
  Wastewater
Anode Contact Cooling And Briquette Quenching
  Water
Cathode Manufacturing
Cathode Reprocessing
Potline Wet Air Pollution Control Wastewater
Potline SO2 Wet Air Pollution Control
Potroom Wet Air Pollution Control Wastewater
753

753
753
753
754
754
754
755
755
755
756

759

761
                                                           761
                                                           762
                                                           763
                                                           763

                                                           764

                                                           764
                                                           764
                                                           764
                                                           764
                                                           766
                                                           766
                                                           767
                                                           768
                                                           770
                                                           771

                                                           771

                                                           772

                                                           773
                                                           773
                                                           774
                                                           775
                                                           775
                                595

-------
                  PRIMARY ALUMINUM  SUBCATEGORY
                   TABLE OP CONTENTS  (Continued)
 Section

 X
 (Cont'd)
XI
XII
XIII
Pot Repair And Pot Soaking                       776
Degassing Wet Air Pollution Control              777
Direct Chill Casting Contact Cooling             777
Continuous Rod Casting Contact Cooling           777
Statuonary Casting Contact Cooling               778
Shot Casting Contact Cooling                     778
Regulated Pollutant Parameters                   778
Effluent Limitations                             781

NEW SOURCE PERFORMANCE STANDARDS                 881

Technical Approach To BDT                        813
Option A                                         813
Option B                                         813
Option C                                         814
Option E                                         814
BDT Option Selection                             814
Regulated Pollutant Parameters                   816
New Source Performance Standards                 816

PRETREATMENT STANDARDS                           835

Technical Approach To Pretreatment               835
Pretreatment Standards For Existing Sources      836
Pretreatment Standards For New Sources           836
Option A                                         836
Option B                                         836
Option C                                         837
Option E                                         837
PSNS Option Selection                            837
Regulated Pollutant Parameters                   837
Pretreatment Standards                           838

BEST CONVENTIONAL POLLUTANT CONTROL TECHNOLOGY   855
                               596

-------
                 PRIMARY ALUMINUM SUBCATEGORY
                         LIST OF TABLES
Table              Title                              Page

III-l     Initial Operating Years (Range) Summary of       638
             Plants in the Primary Aluminum Subcategory
             by Discharge Type

III-2     Production Ranges for the Primary Aluminum       639
             Subcategory

III-3     Summary of Subcategory Processes and             640
             Associated Waste Streams

IV-1      Production Normalizing Parameters                647

V-l       Water Discharge Rates for Anode                  659
            a.nd Cathode Paste Plant Wet
            Air Pollution Control (1/kkg)

V-2       Primary Aluminum Sampling Data                   660
            Anode Paste Plant Wet Air
            Pollution Control Raw Wastewater

V-3       Water Discharge Rates for Anode                  662
            Bake Plant Wet Air Pollution
            Control (1/kkg of Anodes Baked)

V-4       Primary Aluminum Sampling Data                   663
            Anode Bake Plant Scrubber
            Liquor Raw Wastewater

V-5       Water Discharge Rates for Anode                  665
            Contact Cooling and Briquette
            Quenching (1/kkg of Green
            Anodes or Briquettes Manufactured)

V-6       Primary Aluminum Sampling Data                   666
            Paste Plant Contact Cooling
            Water Raw Wastewater

V-7       Water Discharge Rates for                    ,    668
            Cathode Reprocessing
            (1/kkg of Cryolite Production)

V-8       Primary Aluminum Sampling Data                   669
            Cathode Reprocessing Raw  Wastewater

V-9       Water Discharge Rates for                        784
            Potline Wet Air Pollution
            Control (1/kkg of Aluminum
            Reduction Production)
                               597

-------
                  PRIMARY ALUMINUM SUBCATEGORY
          LIST OF TABLES (Continued)
 Table    Title

 V-10      Primary Aluminum Sampling Data
             Potline Wet Air Pollution
             Control Raw Wastewater

 V-ll      Water Discharge Rates for
             Potline S02 Wet Air
             Pollution Control (1/kkg of
             Aluminum Reduced)

 V-12      Water Discharge Rates for
             Potroom Wet Air Pollution
             Control (1/kkg of Aluminum
             Reduction Production)

 V-13      Primary Aluminum Sampling Data
             Potroom Wet Air Pollution
             Control Raw Wastewater

 V-14      Water Discharge Rates for
             Degassing Wet Air Pollution
             Control (1/kkg of Aluminum
             Refined and Degassed)

 V-15      Primary Aluminum Sampling Data
             Refining and Degassing Wet
             Air Pollution Control  Raw
             Wastewater

 V-16      Water Discharge Rates  for Pot
             Repair-Pot Soaking (1/kkg of
             Aluminum Reduction Production)

 V-17      Water Discharge Rates  for Direct
             Chill  Casting Contact  Cooling
             (Primary Aluminum Subcategory)
             (1/kkg of Aluminum Cast)

 V-18      Water Discharge Rates  for Direct
             Chill  Casting Contact  Cooling
             (Aluminum Forming  Category)

 V-19       Water  Discharge  Rates  for
             Continuous Rod Casting
             Contact  Cooling
             (1/kkg of Aluminum Cast)

V-20      Primary Aluminum Sampling Data
             Casting  Contact Cooling
            Water Raw Wastewater
675
    679
    680
    681
    686
    687
    688
   689
   690
   692
   693
                               598

-------
                 PRIMARY ALUMINUM SUBCATEGORY
         LIST OF TABLES (Continued)
Table    Title                              Page

V-21      Primary Aluminum Sampling Data
            Miscellaneous Wastewater

V-22      Primary Aluminum Sampling Data
            Treatment Plant Samples -
            Plant A

V-23      Primary Aluminum Sampling Data
            Treatment Plant Samples -
            Plant B

V-24      Primary Aluminum Sampling Data
            Treatment Plant Samples -
            Plant C

V-25      Primary Aluminum Sampling Data
            Treatment Plant Samples -
            Plant D

V-26      Primary Aluminum Sampling Data
            Treatment Plant Samples -
            Plant E

V-27      Primary Aluminum Sampling Data
            Treatment Plant Samples -
            Plant F

V-28      Reported Presence or Absence of
            Toxic Pollutants

V-29      Source Water Characteristics

V-30      Raw Wastewater Characteristics -
            Potli-ne  Scrubber Slowdown

V-31      Concentration of PAH in  Potline
            Raw Wastewater

V-32      Sample Data Summary for  PAH
            Analysis in Potline  Scrubber Liquor
            - Clarifier Effluent,  Filter Effluent,
            and Carbon Adsorption  Effluent

V-33      Sample Data Summary for  Metal
            Removal  in Potline Scrubber Liquor
            - Clarifier and Filter Effluent

VI-1      Frequency  of Occurrence  of
            Toxic Pollutants Primary
            Aluminum Raw Wastewater
695


701



702



704



706



708



710



712


713

714


715


716





717



735
                                599

-------
                  PRIMARY  ALUMINUM SUBCATEGORY
          LIST  OF  TABLES  (Continued)
 Table

 VI-2

 VI-3


 VI-4


 VIII-1
X-l
X-2
X-3
Title

 Toxic Pollutants Never Detected
Page
X-4
X-5
X-6
X-7
XI-1
 Toxic Pollutants Never Found Above Their
     Analytical Quantification Level

 Toxic Pollutants Detected in a Small
     Number of Sources

 Cost of Compliance for the
   Primary Aluminum Subcategory
   Direct Dischargers (March
   1982 - Millions of Dollars)

 Current Recycle Practices
   Within the Primary
   Aluminum Subcategory

 Pollutant Removal Estimates
   for Primary Aluminum Direct
   Dischargers Toxic Organics

 Pollutant Removal Estimates for
   Primary Aluminum Direct
   Dischargers Inorganics -
   Combined Metals Data Base
   (CMDB)

 Pollutant Removal Estimates for
   Primary Aluminum Direct
   Dischargers Inorganics -
   Alternate -Data Base

 Pollutant Removal Estimates for
   Primary Aluminum Inorganics -
   Total

 BAT Wastewater Discharge Rates
   for the Primary Aluminum
   Subcategory

 BAT Effluent  Limitations for
   the Primary Aluminum
   Subcategory

 Plants Currently Manufacturing
   or Capable  of Manufacturing
   High Purity Alloys  Using
   Alternate In-Line Fluxing
   and Filtering
               739

               741


               742


               757





               782



               783



               784
               785
               786
               787
               789
               818
                               600

-------
                 PRIMARY ALUMINUM SUBCATEGORY
         LIST OF TABLES (Continued)
Table    Title

XI-2      NSPS Wastewater Discharge Rates
            for the Primary Aluminum
            Subcategory

XI-3      NSPS for the Primary Aluminum
            Subcategory

XII-1     PSNS Wastewater Discharge Rates
            for the Primary Aluminum
            Subcategory

XII-2     PSNS for the Primary Aluminum
                      Subcategory
Paqe
               819



               821


               839



               841
                                601

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                  PRIMARY ALUMINUM SUBCATEGORY
                         LIST OF FIGURES
Figure              Title
III-l     Primary Aluminum Reduction Process
III-2     Geographic Locations of Primary Aluminum
             Reduction Plants
V-l       Sampling Sites at Primary Aluminum Plant A
V-2       Sampling Sites at Primary Aluminum Plant B
V-3       Sampling Sites at Primary Aluminum Plant C
V-4       Sampling Sites at Primary Aluminum Plant D
V-5       Sampling Sites at Primary Aluminum Plant E
V-6       Sampling Sites at Primary Aluminum Plant F
X-l       BAT Treatment Scheme Option A
              Primary Aluminum Subcategory
X-2       BAT Treatment Scheme Option B
              Primary Aluminum Subcategory
X-3       BAT Treatment Scheme Option C
              Primary Aluminum Subcategory
X-4       BAT Treatment Scheme Option E
              Primary Aluminum Subcategory
Page
    641
    642

    718
    719
    720
    721
    722
    723
    808

    809

    810

    811
                               602

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               PRIMARY ALUMINUM SUBCATEGORY   SECT - I




                            SECTION I

                     SUMMARY AND CONCLUSIONS
On  April  8,  1974,  EPA promulgated  technology-based  effluent
limitations  guidelines and performance standards for the primary
aluminum  smelting subcategory of the Nonferrous Metals  Manufac-
turing Point Source Category.  This regulation included BPT, BAT,
NSPS,  and PSNS limitations.  EPA promulgated amendments to  BAT,
NSPS, and PSNS for this subcategory pursuant to the provisions of
the Clean Water Act Amendments of 1977. This supplement  provides
a  compilation  and analysis of the background material  used  to
develop these amended effluent limitations and standards.

On  March 8, 1984 (49FR8742) EPA promulgated final amendments  to
40  CFR Part 421, substantially revising BAT limitations and  new
source and pretreatment standards for both primary and  secondary
aluminum  smelting. After promulgation of these  amendments,  the
Aluminum   Association,  Kaiser  Aluminum  and  Chemical   Corp.,
Reynolds Metals Company, the Aluminum Recycling Association,  and
others filed petitions to review the regulation. In November 1985
these  four parties entered into two settlement agreements  which
resolved issues raised by the petitioners related to the  primary
aluminum  and  secondary aluminum subcategories.   In  accordance
with  these  Settlement  Agreements, EPA published  a  notice  of
proposed rulemaking on May  20, 1986 and solicited comments.

EPA  then promulgated final amendments to the regulation for  the
Primary  Aluminum   Subcategory   on July 7, 1987  (52  FR   25552)
concerning four topics, which are summarized here.

The  BAT limitations     for benzo(a)pyrene were amended  in  two
respects:  first,   to  incorporate  variability factors  into  the
daily  maximum and  monthly  average limitations;  and   second,  to
only  provide  discharge allowances for benzo(a)pyrene  to  those
processes which generate this substance.   Further, clarification
is provided on-2 items related to regulation of benzo(a)pyrene.

The BAT limitations and NSPS and PSNS  for fluoride are amended to
be based upon the pooled variability factors calculated  from data
for  seven  metal pollutants in the combined  metals   data  base,
namely  4.10  and   1.82  for the daily and  monthly   variability
factors,  respectively.   This  amendment  was  made   because_ of
petitioners  concerns about  the presence of complex fluoride ions
and aluminum salts  in  the wastewater.

Brief  guidance   is provided on the treatment values that   permit
writers may  provide for spent potliner leachate,  even though EPA
considers   spent  potliner   leachate   to  be  a  non-process  and
therefore a  non-scope  flow.

The  NSPS pH standards  for  direct chill, casting  contact cooling
water are amended  to a  range of  6.0  to 10.0  standard units  at all
                                603

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                 PRIMARY ALUMINUM  SUBCATEGORY   SECT - I
  times.
 The  primary aluminum subcategory is comprised of 31 plants.   Of
 the  31  plants,   24 discharge  directly  to  rivers,  lakes,  or
 streams; none discharge to publicly owned treatment works  (POTW);
 and seven achieve  zero discharge of process wastewater.

 EPA  first examined the primary aluminum subcategory to determine
 whether differences in raw materials, final products, manufactur-
 ing processes, equipment, age and size of plants, and water usage
 required  the  development of separate effluent  limitations  and
 standards  for  different  segments  of  the  subcategory.   This
 involved a detailed analysis of wastewater discharge and  treated
 effluent characteristics, including (1) the sources and volume of
 water used, the processes employed, and the sources of pollutants
 and wastewaters in the plant; and (2) the constituents of waste-
 waters, including toxic pollutants.

 Several  distinct  control and treatment technologies  (both  in-
 plant  and  end-of-pipe)   applicable  to  the  primary   aluminum
 subcategory  were identified.   The Agency analyzed both histori-
 cal and newly generated data on the performance of these technol-
 ogies,   including  their  nonwater quality  environmental  impacts
 (air_  quality  impacts  and solid waste  generation)   and  energy
 requirements.   EPA also studied various flow reduction techniques
 reported  in  the  data  collection portfolios  (dcp)   and  plant
 visits.

 Engineering  costs  were   prepared for  each  of  the   control  and
 treatment   options considered for the subcategory.    These  costs
 were  then  used  by the  Agency to estimate the impact of  implement-
 ing  the various  options  on the industry.    For  each  control  and
 treatment   option that the Agency found to be  most effective  and
 technically feasible in controlling  the discharge of  pollutants,
 the ^number of  potential  closures,   number of  employees  affected,
 and impact  on price were  estimated.   These  results are   reported
 in  a  separate document entitled "The Economic  Impact Analysis  of
 Effluent Limitations  and  Guidelines   and  Standards   for    the
 Nonferrous  Smelting and Refining  Industry".

 Based on consideration of  the above  factors, EPA  identified  vari-
 ous control and treatment  technologies  which formed the basis  for
 BAT and selected  control  and treatment  appropriate for each  set
 of  standards and limitations.   The mass  limitations and standards
 for BAT, NSPS, and  PSNS are presented in Section  II.

 For_BAT, the Agency  has built upon the BPT basis  of lime precipi-
 tation   and sedimentation  by  adding  in-process control  technolo-
 gies  which include  recycle of process water from air  pollution
 control and metal contact  cooling waste streams.   Filtration  is
 added  as  an effluent polishing step to further  reduce  metals,
 toxic  organics, and suspended solids concentrations.   In   addi-
 tion, cyanide precipitation is added to control cyanide.  To meet
 the  BAT  effluent  limitations based  on  this   technology,  the
primary  aluminum  smelting subcategory is estimated to  incur  a
                               604

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               PRIMARY ALUMINUM SUBCATEGORY   SECT
capital cost of $10.5 million (March, 1982 dollars) and an annual
cost of $16 million (March, 1982 dollars).

The  best demonstrated technology (BDT),  which is the  technical
basis of NSPS,  is equivalent to BAT for most waste streams.   In
selecting BDT,  EPA recognizes that new plants have the  opportu-
nity to implement the best and most efficient manufacturing pro-
cesses and treatment technology.   As such,  the technology basis
of  NSPS  for the removal of toxic organics present  in  scrubber
wastewater  from anode paste plants,  anode bake plants,  and pot
lines,  is dry alumina air pollution scrubbing systems.   Potroom
scrubbing  is eliminated based on efficient capture of  emissions
with potline scrubbers.   Degassing wet air pollution control  is
eliminated  through in-line fluxing and filtering.   Treatment of
toxic metals and toxic organics is based upon lime precipitation,
sedimentation,  and  filtration.   Cyanide precipitation  is  the
basis  for the control of cyanide,  and oil skimming is  included
for the control of oil and grease.

The Agency is not promulgating pretreatment standards for exist-
ing sources (PSES) since there are no indirect discharging plants
in  the primary aluminum subcategory.   The technology basis  for
pretreatment standards for new sources (PSNS) is the best demon-
strated  technology, and   the PSNS are identical to NSPS for  all
building blocks.
                               605

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PRIMARY ALUMINUM SUBCATEGORY
SECT - I
THIS PAGE INTENTIONALLY LEFT BLANK
                606

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               PRIMARY ALUMINUM SUBCATEGORY   SECT - II
                            SECTION II

                         RECOMMENDATIONS

EPA  has  divided  the  primary  aluminum  subcategory  into   12
subdivisions  or  building  blocks for the  purpose  of  effluent
limitations and standards.  These building blocks are:

     (a)  Anode and cathode paste plant wet air pollution control
     (b)  Anode bake plant wet air pollution control
     (c)  Cathode reprocessing
     (d)  Anode and briquette contact cooling
     (e)  Potline wet air pollution control
     (f)  Potline SO2 wet air pollution control
     (g)  Potroom wet air pollution control
     (h)  Degassing wet air pollution control
     (i)  Pot repair and pot soaking
     (j)  Direct chill casting contact cooling
     (k)  Continuous rod casting contact cooling
     (1)  Stationary and shot casting contact cooling

EPA promulgated BPT, BAT, NSPS, and PSNS effluent limitations for
the primary aluminum subcategory on April 8, 1974 as Subpart B of
40  CFR  Part 421.  Unlike this rulemaking, the  limitations  and
standards  were  developed  for  the  entire  aluminum   smelting
process, not on the basis of individual building blocks.  BPT was
promulgated  based on effluent concentrations achievable  by  the
application of chemical precipitation and sedimentation (lime and
settle) technology and average process wastewater flowrates.  For
this rulemaking, EPA is not modifying these BPT limitations.

The following BPT effluent limitations were promulgated:
   Pollutant or
Pollutant Property
Maximum for
Any One Day
  Maximum for
Monthly Average
                 Metric Units - kg/kkg of product
            English Units - lbs/1,000 Ibs of product
Fluoride
Total Suspended Solids
pH
     2.0              1.0
     3.0              1.5
Within the range of £ to 9
         at all times
EPA  is  modifying  the BAT effluent  limitations  to  take  into
account pollutant concentrations achievable by the application of
chemical precipitation, sedimentation, and multimedia  filtration
(lime,  settle,  and  filter)  technology  and  in-process   flow
reduction  control  methods,  along  with  preliminary  treatment
consisting  of  cyanide precipitation with  ferrous  sulfate  for
                               607

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                PRIMARY ALUMINUM SUBCATEGORY   SECT  -  II


 selected   waste streams.   The  following BAT effluent   limitations
 are  promulgated for  existing sources:

 (a)  Anode and  Cathode Paste Plant  Wet  Air  Pollution  Control  BAT
   Pollutant  or
Pollutant  Property
Maximum for
Any One Day
  Meiximum for
Monthly Average
             Metric Units  - mg/kg  of  paste  produced
         English Units  -  Ibs/million Ibs  of  paste produced
Benzo(a)pyrene
Antimony
Nickel
Aluminum
Fluoride
      0.005
      0.263
      0.075
      0.831
      8.092
       0.002
       0.117
       0.050
       0.369
       3.591
 (b)  Anode Contact Cooling and Briquette Quenching BAT
   Pollutant or
Pollutant Property
Maximum for
Any One Day
  Maximum for
Monthly Average
               Metric Units - mg/kg of anodes cast
          English Units - Ibs/million Ibs of anodes cast
Benzo(a)pyrene
Antimony
Nickel
Aluminum
Fluoride
      0.007
      0.403
      0.115
      1.277
     12.440
       0.003
       0.180
       0.077
       0.566
       5.518
(c)  Anode Bake Plant Wet Air Pollution Control  (Closed top
     ring furnace) BAT
   Pollutant or
Pollutant Property
Maximum for
Any One Day
  Maximum for
Monthly Average
               Metric Units - mg/kg of anodes baked
          English Units - Ibs/million Ibs of anodes baked
Benzo(a)pyrene
Antimony
Nickel
Aluminum
Fluoride
      0.146
      8.346
      2.378
     26.420
    257.300
       0.067
       3.719
       1.600
      11.720
     114.200
                               608

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               PRIMARY ALUMINUM SUBCATEGORY   SECT - II
(d)  Anode Bake Plant Wet Air Pollution Control (Open top
     ring furnace with spray tower only) BAT
   Pollutant or
Pollutant Property
Maximum for
Any One Day
  Maximum for
Monthly Average
               Metric Units - mg/kg of anodes baked
         English Units - Ibs/million Ifos of anodes baked
Benzo(a)pyrene
Antimony
Nickel
Aluminum
Fluoride
      0.002
      0.097
      0.028
      0.306
      2.975
       0.001
       0.043
       0.019
       0.136
       1.320
(e)  Anode Bake Plant Wet Air Pollution. Control (Open top rim
     furnace with wet electrostatic precipitator and spray
     tower) BAT
   Pollutant or
Pollutant Property
Maximum for
Any One Day
  Maximum for
Monthly Average
               Metric Units - mg/kg of anodes baked
         English Units - Ibs/million Ibs of anodes baked
Benzo(a)pyrene
Antimony
Nickel
Aluminum
Fluoride
      0.025
      1.409
      0.402
      4.461
     43.440
       0.011
       0.628
       0.270
       1.979
      19.270
(f)  Anode Bake Plant Wet Air Pollution Control (Tunnel kiln) BAT
   Pollutant or
Pollutant Property
Maximum for
Any One Day
  Maximum for
Monthly Average
               Metric Units - mg/kg of anodes baked
         English Units - Ibs/million Ibs of anodes baked
Benzo(a)pyrene
Antimony
Nickel
Aluminum
Fluoride
      0.038
      2.197
      0.626
      6.953
     67.710
       0.018
       0.979
       0.421
       3.084
      30.050
                               609

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               PRIMARY ALUMINUM SUBCATEGORY   SECT - II
(g)  Cathode Reprocessing (Operated with dry potline scrubbing
     and not commingled with other process or nonprocess
     waters) BAT
   Pollutant or
Pollutant Property
Maximum for
Any One Day
  Maximum for
Monthly Average
           Metric   Units   -   mg/kg   of   cryolite
English Units - Ibs/million Ibs of cryolite recovered
Benzo(a)pyrene
Antimony
Cyanide
Nickel
Aluminum
Fluoride
      1.181
    420.400
    157.600
     80.570
    273.200
 29,430.000
                      recovered
       0.547
     189.200
      70.060
      35.030
     122.600
  13,310.000
(h)  Cathode Reprocessing (Operated with dry potline scrubbing
     and commingled with other process or nonprocess waters) BAT
   Pollutant or
Pollutant Property
Maximum for
Any One Day
  Maximum for
Monthly Average
            Metric Units - mg/kg of cryolite recovered
      English Units - Ibs/million Ibs of cryolite recovered
Benzo(a)pyrene
Antimony
Cyanide
Nickel
Aluminum
Fluoride
      1.181
     67.610
    157.600
     19.270
    214.000
  2,084.000
       0.547
      30.120
      70.060
      12.960
      94.930
     924.800
(i) Cathode Reprocessing (Operated with wet potline scrubbing) BAT
   Pollutant or
Pollutant Property
Maximum for
Any One Day
  Maximum for
Monthly Average
            Metric Units - mg/kg of cryolite recovered
      English Units - Ibs/million Ibs of cryolite recovered
Benzo(a)pyrene
Antimony
Cyanide
Nickel
Aluminum
Fluoride
      0.000
      0.000
      0.000
      0.000
      0.000
      0.000
       0.000
       0.000
       0.000
       0.000
       0.000
       0.000
                               610

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               PRIMARY ALUMINUM SUBCATEGORY   SECT - II
(j)  Potline Wet Air Pollution Control (Operated without  cathode
     reprocessing) BAT

   Pollutant or
Pollutant Property
Maximum for
Any One Day
  Maximum for
Monthly Average
   Metric Units - mg/kg of aluminum produced from electrolytic
                            reduction
    English Units - Ibs/million Ibs of aluminum produced from
                      electrolytic reduction
Benzo(a)pyrene
Antimony
Nickel
Aluminum
Fluoride
      0.028
      1.618
      0.461
      5.120
     49.860
       0.013
       0.721
       0.310
       2.271
      22.130
(k)  Potline Wet Air Pollution Control (Operated with cathode
     reprocessing and not commingled with other process or
     nonprocess waters) BAT
   Pollutant or
Pollutant Property
Maximum for
Any One Day
  Maximum for
Monthly Average
   Metric Units - mg/kg of aluminum produced from electrolytic
                            reduction
    English Units - Ibs/million Ibs of aluminum produced from
                      electrolytic reduction
Benzo(a)pyrene
Antimony
Cyanide
Nickel
Aluminum
Fluoride
      0.028
     10.060
      3.771
      1.928
      6.537
    703.900
       0.013
       4.525
       1.676
       0.838
       2.993
     318.500
                               611

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               PRIMARY ALUMINUM SUBCATEGORY   SECT - II
(1)  Pofcline Wet Air Pollution Control (Operated with cathode
     reprocessing and commingled with other process or_ nonprocess
     wastewaters) BAT
   Pollutant or
Pollutant Property
Maximum for
Any One Day
  Maximum for
Monthly Average
   Metric Units - mg/kg of aluminum produced from electrolytic
                            reduction
    English Units - Ibs/million Ibs of aluminum produced from
                      electrolytic reduction
Benzo(a)pyrene
Antimony
Cyanide
Nickel
Aluminum
Fluoride
      0.028
      1.618
      3.771
      0.461
      5.120
     49.860
       0.013
       0.721
       1.676
       0.310
       2.271
      22.130
(m)  Potroom Wet Air Pollution Control  BAT
   Pollutant or
Pollutant Property
Maximum for
Any One Day
  Maximum for
Monthly Average
   Metric Units - mg/kg of aluminum produced from electrolytic
                            reduction
    English Units - Ibs/million Ibs of aluminum produced from
                      electrolytic reduction
Benzo(a)pyrene
Antimony
Nickel
Aluminum
Fluoride
      0.056
      3.204
      0.913
     10.140
     98.770
       0.026
       1.428
       0.614
       4.499
      43.830
(n)  Potline SO? Emissions Wet Air Pollution Control  BAT
   Pollutant or
Pollutant Property
Maximum for
Any One Day
  Maximum for
Monthly Average
   Metric Units - mg/kg of aluminum produced from electrolytic
                            reduction
    English Units - Ibs/million Ibs of aluminum produced from
                      electrolytic reduction
Benzo(a)pyrene                          0.045           0.021
Antimony                                2.588           1.153
Cyanide                                 0.738           0.496
Nickel                                  8.194           3
Aluminum
Fluoride
     79.790
         ,634
      35.400
                               612

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               PRIMARY ALUMINUM SUBCATEGORY
            SECT - II
(o)  Degassing Wet Air Pollution Control BAT
   Pollutant or
Pollutant Property
Maximum for
Any One Day
  Maximum for
Monthly Average
   Metric Units - mg/kg of aluminum produced from electrolytic
                            reduction
    English Units - Ibs/million Ibs of aluminum produced from
                      electrolytic reduction
Benzo(a)pyrene
Antimony
Nickel
Aluminum
Fluoride
       (1)
      5.036
      1.435
     15.940
    155.300
        (1)
       2.244
       0.965
       7.071
      68.880
(1)  There shall be no discharge allowance for this pollutant
(p)  Pot Repair and Pot Soaking BAT
   Pollutant or
Pollutant Property
Maximum for
Any One Day
  Maximum for
Monthly Average
   Metric Units - mg/kg of aluminum produced from electrolytic
                            reduction
    English Units - Ibs/million Ibs of aluminum produced from
                      electrolytic reduction
Benzo(a)pyrene
Antimony
Nickel
Aluminum
Fluoride
      0.000
      0.000
      0.000
      0.000
      0.000
       0.000
       0.000
       0.000
       0.000
       0.000
                               613

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                PRIMARY ALUMINUM SUBCATEGORY    SECT  -  II
 (q)   Direct  Chill  Casting  Contact  Cooling  BAT
    Pollutant  or
 Pollutant  Property
               Maximum for
               Any One Day
  Maximum for
Monthly Average
   Metric Units  - mg/kg of aluminum product from direct chill
                             casting
     English Units - Ibs/million Ibs of aluminum product from
                       direct chill casting
Benzo(a)pyrene
Antimony
Nickel
Aluminum
Fluoride
                      (1)
                     2.565
                     0.731
                     8.120
                    79.080
        (1)
       1.143
       0.492
       3.602
      35.090
 (r)  Continuous Rod Casting Contact Cooling  BAT
   Pollutant or
Pollutant Property
               Maximum for
               Any One Day
  Maximum for
Monthly Average
    Metric Units
   English Units
Benzo(a)pyrene
Antimony
Nickel
Aluminum
Fluoride
mg/kg of aluminum product from rod casting
Ibs/million Ibs of aluminum product from rod
          casting
                      (1)
                     0.201
                     0.057
                     0.636
                     6.188
        (1)
       0.089
       0.038
       0.282
       2.746
(1)  There shall be no discharge allowance for this pollutant
                               614

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               PRIMARY ALUMINUM SUBCATEGORY
            SECT - II
(s)  Stationary Casting or Shot Casting Contact Cooling BAT
   Pollutant or
Pollutant Property
Maximum for
Any One Day
  Maximum for
Monthly Average
Metric Units - mg/kg of aluminum product from stationary casting
                         or shot casting
     English Units - Ibs/million Ibs of aluminum product from
                stationary casting or shot casting
Benzo(a)pyrene
Antimony
Nickel
Aluminum
Fluoride
      0.000
      0.000
      0.000
      0.000
      0.000
       0.000
       0.000
       0.000
       0.000
       0.000
EPA  is  modifying  NSPS based  on  the  effluent  concentrations
achievable   by  the  application  of   chemical   precipitation,
sedimentation,  and  multimedia  filtration  (lime,  settle,  and
filter)  technology and elimination of pollutant discharges  from
air  pollution  control through the use of dry  scrubbing,  along
with preliminary treatment consisting of oil skimming and cyanide
precipitation  with ferrous sulfate for selected  waste  streams.
The following effluent standards are promulgated for new sources:


(a)  Anode and Cathode Paste Plant Wet Air Pollution Control NSPS
   Pollutant or
Pollutant Property
Maximum for      Maximum for
Any One Day    Monthly Average
             Metric Units - mg/kg of paste produced
        English Units - Ibs/million Ibs of paste produced
Benzo(a)pyrene
Antimony
Nickel
Aluminum
Fluoride
Oil and Grease
TSS
pH
      0.000           0.000
      0.000           0.000
      0.000           0.000
      0.000           0.000
      0.000           0.000
      0.000           0.000
      0.000           0.000
Within the range of 7.0 to 10.
         at all times
                               615

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                PRIMARY ALUMINUM SUBCATEGORY    SECT  -  II
 (b)  Anode  Contact  Cooling  and  Briquette Quenching NSPS
    Pollutant  or
Pollutant  Property
Maximum  for
Any One  Day
  Maximum for
Monthly Average
               Metric Units - mg/kg of anodes cast
          English Units -  Ibs/million Ibs of anodes cast
Benzo(a)pyrene
Antimony
Nickel
Aluminum
Fluoride
Oil and Grease
TSS
pH
      0.007
      0.403
      0.115
      1.277
     12.440
      2.090
      3.135
       0.003
       0.180
       0.077
       0.566
       5.518
       2.090
       2.508
Within the range of 7.0 to 10.0
         at all times
 (c)  Anode Bake Plant Wet Air Pollution Control NSPS
   Pollutant or
Pollutant Property
Maximum for
Any One Day
  Maximum for
Monthly Average
               Metric Units - mg/kg of anodes baked
         English Units - Ibs/million Ibs of anodes baked
Benzo(a)pyrene
Antimony
Nickel
Aluminum
Fluoride
Oil and Grease
TSS
pH
      0.000           0.000
      0.000           0.000
      0.000           0.000
      0.000           0.000
      0.000           0.000
      0.000           0.000
      0.000           0.000
Within the range of 7.0 to 10.0
         at all times
                               616

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               PRIMARY ALUMINUM SUBCATEGORY
            SECT - II
(d)  Cathode Reprocessing NSPS (Operated with dry potline scrubbing
     and not commingled with other process or nonprocess waters)
   Pollutant or
Pollutant Property
Maximum for
Any One Day
  Maximum for
Monthly Average
            Metric Units - mg/kg of cryolite recovered
      English Units - Ibs/million Ibs of cryolite recovered
Benzo(a)pyrene
Antimony
Cyanide
Nickel
Aluminum
Fluoride
Oil and Grease
TSS
pH
      1.181
    420.400
    157.600
     80.570
    273.200
 29,430.000
    350.300
  2,172.000
       0.547
     189.200
      70.060
      35.030
     122.600
  13,310.000
     350.300
     945.800
Within the range of 7.0 to  10.0
         at all times
 (e)  Cathode Reprocessing NSPS  (Operated with dry potline scrubbing
    and commingled with other process or nonprocess waters)
   Pollutant or
Pollutant Property
Maximum  for
Any One  Day
  Maximum  for
Monthly Average
            Metric Units - mg/kg of cryolite  recovered
       English Units -  Ibs/million  Ibs of cryolite  recovered
 Benzo(a)pyrene
 Antimony
 Cyanide
 Nickel
 Aluminum
 Fluoride
 Oil  and Grease
 TSS
 pH
       1.181           0.547
      67.610          30.130
     157.600          70.060
      19.270          12.960
     214.000          94.930
   2,084.000         924.800
     350.300         350.300
   2,172.000         945.800
 Within the range of 7.0 to 10,
           at all times
                                617

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                PRIMARY ALUMINUM SUBCATEGORY   SECT - II
 (f)   Potline Wet Air Pollution Control NSPS
    Pollutant or
 Pollutant Property
 Maximum for
 Any One Day
  Maximum for
Monthly Average
    Metric Units  - mg/kg  of  aluminum produced  from electrolytic
                             reduction
     English Units -  Ibs/million  Ibs of  aluminum  produced  from
                       electrolytic  reduction
 Benzo(a)pyrene
 Antimony
 Nickel
 Aluminum
 Fluoride
 Oil and Grease
 TSS
 pH
       0.000            0.000
       0.000            0.000
       0.000            0.000
       0.000            0.000
       0.000            0.000
       0.000            0.000
       0.000            0.000
Within the range of 7.0 to 10.0
         at all times
 (g)  Potroom Wet Air Pollution Control NSPS
   Pollutant or
Pollutant Property
Maximum for
Any One Day
  Maximum for
Monthly Average
   Metric Units - mg/kg of aluminum produced from electrolytic
                            reduction
    English Units - Ibs/million Ibs of aluminum produced from
                      electrolytic reduction
Benzo(a)pyrene
Antimony
Cyanide
Nickel
Aluminum
Fluoride
Oil and Grease
TSS
pH
      0.000           0.000
      0.000           0.000
      0.000           0.000
      0.000           0.000
      0.000           0.000
      0.000           0.000
      0.000           0.000
      0.000           0.000
Within the range of 7.0 to 10.0
         at all times
                               618

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               PRIMARY ALUMINUM SUBCATEGORY   SECT - II
(h)  Potline SO? Emissions Wet Air Pollution Control NSPS
   Pollutant or
Pollutant Property
Maximum for
Any One Day
  Maximum for
Monthly Average
   Metric Units - mg/kg of aluminum produced from electrolytic
                            reduction
    English Units - Ibs/million Ibs of aluminum produced from
                      electrolytic reduction
Benzo(a)pyrene
Antimony
Nickel
Aluminum
Fluoride
Oil and Grease
Total Suspended Solids
pH
      0.045
      2.588
      0.738
      8.194
     79.790
       0.021
       1.153
       0.496
       3.634
      35.400
      13.410
      16.090
     13.410
     20.120
Within the range of 7.0 to 10.0
          at all times
(i)  Degassing Wet Air Pollution Control NSPS
   Pollutant or
Pollutant Property
Maximum for
Any One Day
  Maximum for
Monthly Average
   Metric Units - mg/kg of aluminum produced from electrolytic
                             reduction
    English Units - Ibs/million  Ibs of aluminum produced from
                      electrolytic reduction
Benzo(a)pyrene
Antimony
Nickel
Aluminum
Fluoride
Oil and Grease
TSS
pH
       0.000
       o.poo
       0.000
       0.000
       0.000
       0.000
       0.000
        0.000
        0.000
        0.000
        0.000
        0.000
        0.000
        0.000
 Within the  range  of  7.0  to  10.0
          at all times
                                619

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                 PRIMARY ALUMINUM  SUBCATEGORY
             SECT -II
  (j)  Pot Repair and Pot Soaking NSPS
    Pollutant or
 Pollutant Property
 Maximum for
 Any One Day
   Maximum for
 Monthly Average
    Metric Units - mg/kg of aluminum produced from electrolytic
                              refining
     English Units - Ibs/million Ibs of aluminum produced from
                       electrolytic reduction
 Benzo(a)pyrene
 Antimony
 Nickel
 Aluminum
 Fluoride
 Oil and Grease
 TSS

 pH
       0.000
       0.000
       0.000
       0.000
       0.000
       0.000
       0.000
        0.000
        0.000
        0.000
        0.000
        0.000
        0.000
        0.000
Within the range of 7.0 to 10.0
          at all times
 (k)   Direct Chill Casting Contact Cooling NSPS
    Pollutant or
 Pollutant Property
Maximum for
Any One Day
  Maximum for
Monthly Average
    Metric Units  -  mg/kg  of  aluminum product  from direct  chill
                              casting
      English  Units -  Ibs/million  Ibs of aluminum product from
                       direct chill casting
Benzo(a)pyrene
Antimony
Nickel
Aluminum
Fluoride
Oil and Grease
TSS
pH
       (1)
      2.565
      0.731
      8.120
     79.080
     13.290
     19.940
       (2)
        (1)
       1.143
       0.492
       3.602
      35.090
      13.290
      15.950
        (2)
(1)  There shall be no discharge allowance for this pollutant.

(2)   The pH shall be maintained within the range of 7.0 to  10.0
at  all  times  except for those situations when  this  waste  is
discharged  separately  and without commingling  with  any  other
wastewater  in which case the pH shall be within the range of 6.0
to 10.0 at all times.
                               620

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               PRIMARY ALUMINUM SUBCATEGORY   SECT - II
(1)  Continuous Rod Casting Contact Cooling NSPS
   Pollutant or
Pollutant Property
                            Maximum for
                            Any  One Day
  Maximum for
Monthly Average
    Metric Units - mg/kg of aluminum product from rod casting
     English Units - Ibs/million Ibs of aluminum product from
                           rod casting
Benzo(a)pyrene
Antimony
Nickel
Aluminum
Fluoride
Oil and Grease
TSS
pH
                                    (1)
                                   0.201
                                   0.057
                                   0.636
                                   6.188
                                   1.040
                                   1.560
        (1)
       0.089
       0.038
       0.282
       2.746
       1.040
       1.248
                             Within the range of 7.0 to 10.0
                                      at all times
 (m)
Stationary Casting or_ Shot Casting Contact Cooling NSPS
   Pollutant or
Pollutant Property
                             Maximum for
                             Any One Day
  Maximum for
Monthly Average
Metric Units  - mg/kg  of  aluminum product  from  stationary  casting
                          or  shot casting
      English  Units  -  Ibs/million Ibs  of aluminum product  from
                 stationary casting  or shot  casting
 Benzo(a)pyrene
 Antimony
 Nickel
 Aluminum
 Fluoride
 Oil and Grease
 TSS
 pH
                                   0.000           0.000
                                   0.000           0.000
                                   0.000           0.000
                                   0.000           0.000
                                   0.000           0.000
                                   0.000           0.000
                                   0.000           0.000
                             Within the range of 7.0 to 10.0
                                      at all times
 EPA  is  not  promulgating pretreatment  standards  for  existing
 sources  (PSES) for the primary aluminum subcategory since  there
 are no existing indirect dischargers.

 EPA  is  modifying  PSNS based  on  the  effluent  concentrations
 achievable   by  the  application  of   chemical   precipitation,
 •sedimentation,  and  multimedia  filtration  (lime,  settle,  and
                                621

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                PRIMARY ALUMINUM SUBCATEGORY   SECT - II
 filter)   technology  and  elimination  of   pollutant    discharges
 through   the   use   of  dry  scrubbing,   along   with    preliminary
 treatment  consisting  of   cyanide   precipitation  with   ferrous
 sulfate   for  selected waste streams.  The  following   pretreatment
 standards are promulgated  for  new sources:
 (a)  Anode  and  Cathode  Paste  Plant Wet Air  Pollution Control  PSNS
   Pollutant  or
Pollutant Property
Maximum for
Any One Day
  Maximum for
Monthly Average
             Metric Units  - mg/kg of paste produced
        English Units -  Ibs/million Ibs of paste produced
Benzo(a)pyrene
Nickel
Fluoride
      0.000
      0.000
      0.000
       0.000
       0.000
       0.000
 (b)  Anode Contact Cooling and Briquette Quenching PSNS
   Pollutant or
Pollutant Property
Maximum for
Any One Day
  Maximum for
Monthly Average
               Metric Units - mg/kg of anodes cast
          English Units - Ibs/million Ibs of anodes cast
Benzo(a)pyrene
Nickel
Fluoride
      0.007
      0.115
     12.440
       0.003
       0.077
       5.518
(c)  Anode Bake Plant Wet Air Pollution Control PSNS
   Pollutant or
Pollutant Property
Maximum for
Any One Day
  Maximum for
Monthly Average
              Metric Units - mg/kg of anodes baked
         English Units - Ibs/million Ibs of anodes baked
Benzo(a)pyrene
Nickel
Fluoride
      0.000
      0.000
      0.000
       0.000
       0.000
       0.000
                               622

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               PRIMARY ALUMINUM SUBCATEGORY   SECT - II
(d)  Cathode Reprocessing PSNS (Operated with dry potline scrubbing
     and not commingled with other process or nonprocess waters)
   Pollutant or
Pollutant Property
Maximum for
Any One Day
  Maximum for
Monthly Average
            Metric Units - mg/kg of cryolite recovered
      English Units - Ibs/million Ibs of cryolite recovered
Benzo(a)pyrene
Cyanide
Nickel
Fluoride
      1.181
    157.600
     80.570
 29,430.000
       0.547
      70.060
      35.030
  13,310.000
(e)  Cathode Reprocessing PSNS (Operated with dry potline
     scrubbing and commingled with other process or nonprocess
     waters)
   Pollutant or
Pollutant Property
Maximum for
Any One Day
  Maximum for
Monthly Average
            Metric Units - mg/kg of cryolite recovered
      English Units - Ibs/million Ibs of cryolite recovered
Benzo(a)pyrene
Cyanide
Nickel
Fluoride
      1.181
    157.600
     19.270
  2,084.000
       0.547
      70.060
      12.960
     924.800
(f)  Potline Wet Air Pollution Control PSNS
   Pollutant or
Pollutant Property
Maximum for
Any One Day
  Maximum for
Monthly Average
   Metric Units - mg/kg of aluminum produced from electrolytic
                            reduction
    English Units - Ibs/million Ibs of aluminum produced from
                      electrolytic reduction
Benzo(a)pyrene
Nickel
Fluoride
      0.000
      0.000
      0.000
       0.000
       0.000
       0.000
                               623

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               PRIMARY ALUMINUM SUBCATEGORY   SECT -II
(g)  Potroom Wet Air Pollution Control PSNS
   Pollutant or
Pollutant Property
Maximum for
Any One Day
  Maximum for
Monthly Average
   Metric Units - mg/kg of aluminum produced from electrolytic
                            reduction
    English Units - Ibs/million Ibs of aluminum produced from
                      electrolytic reduction
Benzo(a)pyrene
Nickel
Fluoride
      0.000
      0.000
      0.000
       0.000
       0.000
       0.000
(h)  Potline SO2 Emissions Wet Air Pollution Control PSNS
   Pollutant or
Pollutant Property
Maximum for
Any One Day
  Maximum for
Monthly Average
   Metric Units - mg/kg of aluminum produced from electrolytic
                            reduction
      English Units - Ibs/million Ibs of aluminum produced from
                      electrolytic reduction
Benzo(a)pyrene
Nickel
Fluoride
      0.045
      0.738
     79.790
       0.021
       0.496
      35.400
(i)  Degassing Wet Air Pollution Control PSNS
   Pollutant or
Pollutant Property
Maximum for
Any One Day
  Maximum for
Monthly Average
   Metric Units - mg/kg of aluminum produced from electrolytic
                            reduction
    English Units - Ibs/million Ibs of aluminum produced from
                      electrolytic reduction
Benzo(a)pyrene
Nickel
Fluoride
      0.000
      0.000
      0.000
       0.000
       0.000
       0.000
                               624

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               PRIMARY ALUMINUM SUBCATEGORY   SECT - II
(j)  Pot Repair and Pot Soaking PSNS
   Pollutant or
Pollutant Property
Maximum for
Any One Day
  Maximum for
Monthly Average
   Metric Units - mg/kg of aluminum produced from electrolytic
                            reduction
    English Units - Ibs/million Ibs of aluminum produced from
                      electrolytic reduction
Benzo(a)pyrene
Nickel
Fluoride
      0.000
      0.000
      0.000
       0.000
       0.000
       0.000
(k)  Direct Chill Casting Contact Cooling PSNS
   Pollutant or
Pollutant Property
Maximum for
Any One Day
  Maximum for
Monthly Average
   Metric Units - mg/kg of aluminum product from direct chill
                             casting
     English Units - Ibs/million Ibs of aluminum product from
                       direct chill casting
Benzo(a)pyrene
Nickel
Fluoride
       (1)
      0.731
     79.080
        (1)
       0.492
      35.090
(1)  Continuous Rod Casting Contact Cooling PSNS
   Pollutant or
Pollutant Property
Maximum for
Any One Day
  Maximum for
Monthly Average
    Metric Units - mg/kg of aluminum product from rod casting
     English Units - Ibs/million Ibs of aluminum product from
                           rod casting
Benzo(a)pyrene
Nickel
Fluoride
        (1)
      0.057
      6.188
        (1)
       0.038
       2.746
                               625

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               PRIMARY ALUMINUM SUBCATEGORY   SECT - II
(m)  Stationary Casting or Shot Casting Contact Cooling PSNS
   Pollutant or
Pollutant Property
Maximum for
Any One Day
  Maximum for
Monthly Average
Metric Units - mg/kkg of aluminum product from stationary casting
                         or shot casting
     English Units - Ibs/billion Ibs of aluminum product from
                stationary casting or shot casting
Benzo(a)pyrene
Nickel
Fluoride
      0.000
      0.000
      0.000
       0.000
       0.000
       0.000
                               626

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             PRIMARY ALUMINUM SUBCATEGORY
                                            SECT - III
                          SECTION III

                         INDUSTRY PROFILE
This section of the Primary Aluminum Supplement describes the raw
materials  and processes used in reducing alumina to aluminum and
presents  a profile of the primary aluminum plants identified  in
this  study.
DESCRIPTION OF PRIMARY ALUMINUM PRODUCTION

All   primary   aluminum  produced  in  the  United   States   is
manufactured  by  the electrolytic reduction of alumina  via  the
Hall-Heroult  Process.  Figure III-l (page 641) is a  block  flow
diagram  depicting  the  various process steps  involved  in  the
manufacture  of  primary aluminum.  The discussion  that  follows
provides  a  summary  of the processes used in  the  smelting  of
aluminum, with particular emphasis on where water is used.

RAW MATERIALS

The  principal  raw materials used in primary aluminum  reduction
are alumina,  metallurgical or petroleum coke,  pitch,  cryolite,
and  aluminum  fluoride.   Alumina  is  the  product  of  bauxite
refining.
                                                      Process  is
ELECTROLYTIC ALUMINUM PRODUCTION

The  manufacture  of aluminum using the Hall-Heroult
discussed in the following sections.

Reduction Cells

The  electrolytic  cells  used in the  Hall-Heroult  Process  are
called pots.  These pots, ranging in size from 1.8 x 5.5 to 4.3 x
12.8 meters (6 x 18 to 14 x 42 feet),  are made of cast iron  and
lined  with carbon.   This carbon lining serves as the cathode in
the  electrolytic  circuit,  collecting aluminum  ions  from  the
electrolyte.   In the primary aluminum industry, large numbers of
these  pots  (from 100 to 250 cells) are hooked  electrically  in
series.  This forms the potline, the basic production unit of the
reduction plant.   Potlines are generally contained in one or two
long, ventilated buildings called potrooms.

The  electrolyte is a solution of alumina in molten  cryolite,  a
double  fluoride  salt  of  calcium  and  aluminum.   Alumina  is
periodically added to and dissolved in the molten electrolyte  to
maintain  the  alumina concentration.   The cells are  heated  to
about  950°C, and  an  electrical current is passed  through  the
molten  cryolite  to force the aluminum ions to  migrate  to  the
                               627

-------
             PRIMARY ALUMINUM SUBCATEGORY
SECT - III
cathode,   where  they  are  reduced  to  aluminum.    The  molten
aluminum,  because of its heavier weight,   collects  in the bottom
of  the  pot,  forming  a  layer  beneath   the   cryolite-alumina
solution.

The  anode  is the electrical counterpart  of the cathode  in  the
electrolytic  cell.   The  anode  used in   the  primary  aluminum
industry   is  made  from  coal  tar  pitch  and  coke  and  when
electrically connected is given a positive charge.  This positive
charge  attracts  negative  ions  from  the  cryolite   solution,
transferring  the positive charge to the aluminum.   This is  the
manner  in which the positive aluminum ions,  which  are attracted
to the negatively charged cathode, are formed.  Additionally, the
carbon  anode  reacts  with  by-product  oxygen  to   form  carbon
monoxide and carbon dioxide.   Thus, the anode is consumed by the
process  of  charge transfer and must be  replaced  pe-nodically.
Potline  cells are generally operated with currents  ranging  from
80,000  to  100,000 amperes.   Anodes used  in  the   Hall-Heroult
Process are of two basic types:  prebaked and Soderberg anodes.

Fabrication  of prebaked and Soderberg anodes is performed in the
anode paste plant where coal tar pitch and ground petroleum  coke
are  blended together to form a paste.   Prebaked anodes,  as the
name suggests,  are baked prior to their use in the  electrolytic
cell.  Iron rods are then attached to the anode so that it may be
suspended  above the electrolytic cell.   Above the  electrolytic
cell,  the  anodes are assembled in two basic patterns.   In  the
side  worked prebaked cell,  the anodes are assembled in two rows
extending the length of the cell with the rows closely spaced  in
the center of the cell.  This arrangement provides a working area
on  each  side of the cell between the cell side lining  and  the
anodes  where  aluminum is added to the cell  (thus the name  side
worked prebake cell).   In the center worked prebake cell, anodes
are placed in two rows and placed closer to the cell side lining,
providing the working area in the center of the cell between  the
rows   (thus  the  name center worked  prebake  cell).,   In  1984,
prebaked anodes were used in 20 of 31 primary aluminum plants.

The alternative to the prebaked anode is the Soderberg anode.  In
the    Soderberg  process,   the  anode  paste  is  used  in   the
electrolytic  cell  without  prior  processing.    The  paste  is
periodically  fed into a rectangular steel compartment above  the
pot.   The heat of the chemical reaction in the pot then bakes the
paste,   fusing  the new material with the old anode.   The tip of
this anode projects through the steel shell into  the electrolyte.
As  the  tip is oxidized,  constant replacement of the  anode  is
possible. Two configurations exist in the aluminum industry using
the Soderberg process:    (1) the Horizontal Stud  Soderberg   (HSS)
process  and  (2) the Vertical Stud Soderberg  (VSS) process.   The
HSS  system  uses horizontal studs or pins to support  the_ anode
body,  while  the VSS system uses vertical pins.  In the horizontal
Soderberg process, the holding pins are adjusted  from  the side of
the  pot,  while in the vertical  Soderberg process the  pins  are
adjusted from  the top.    Since  the paste is added  from  above,
complete hooding of the VSS cell  is not possible,  and more fumes
                                628

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             PRIMARY ALUMINUM SUBCATEGORY   SECT - III


may be emitted to the potroom than with the use of prebaked anode
cells.   The  VSS  and HSS cell  configurations  were  originally
thought to have a great advantage since they eliminated the  need
for a separate paste plant.  The presence of carbon which has not
been   solidified,  however, has become a problem.   The  unbaked
carbon  paste  which  is added to the anode  gives  off  volatile
organic compounds (VOC).  These VOC emissions may condense in the
ductwork  or  in the air pollution control  equipment  and  cause
fouling.   In  addition,  VOC  and  fluoride  emissions  must  be
controlled simultaneously.

The  prebaked  anode is more expensive to manufacture because  of
the bake plant requirement;  however, it is the most electrically
efficient of the three anode types.   The distribution of  plants
in 1984 with VSS, HSS, and prebaked anodes is listed below:


               Anode Type   Number of Plants
               Prebaked
               VSS
               HSS
20
 4
 7
 It   is  essential  for  purity of the product  aluminum  and  the
 structural   integrity  of the cell that  the  molten  aluminum  be
 isolated  from  the  iron shell.    If the pot was left unlined,  the
 iron would  react with the electrolytic bath, and an iron-aluminum
 alloy  would  be the result of the   electrolysis.   Therefore,  a
 carbon liner is used.  A service life of up to three years may be
 attained  for  a properly installed liner in a well-managed  cell,
 but  an average life of between two and three years is  reported to
 be more common.

 Upon failure of a  liner, the cell is emptied, cooled,  and removed
 from the  cell  room to a working  area.  By mechanical drilling^and
 soaking in  water,  the shell is  stripped of old lining  material,
 which  may   be processed through a cathode reprocessing  -facility
 for  recovery of fluoride values  or simply set aside in a storage
 yard.

 Potline   cells emit  gases  containing  particulates,   fluoride
 compounds,   SOX, COX, tars, and  oils.  Emissions can be  collected
 by   using  hoods   above  the   cells  and  treated  by  wet or  dry
 processes.   Activated alumina adsorption is the most  common  dry
 process;  however,  electrostatic  precipitators are  also used.  Two
 types   of alumina  are used  in  the electrolytic cell:   floury and
 sandy   alumina.    Sandy  alumina  is often used for  air  scrubbing
 prior   to  its use  as a raw material,   while floury   alumina   is
 generally  not used  as a scrubbing material because  it lacks  the
 physical  characteristics that  make a good scrubbing material. The
 alumina adsorption method  allows for recycle of  the  fluoride  back
 to  the cell.   At  the  time  of  the  1974  rulemaking,  wet  pot   line
 air   scrubbing was  the  largest  single  contributor of  pollutants
 (fluoride  and TSS)  to  the plant's  wastewater.    At   that   time,
 'about   88 percent  of the aluminum plants used wet  scrubbing.   In
                                629

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              PRIMARY ALUMINUM  SUBCATEGORY   SECT - III


 contrast,  only 35 percent of  the plants are now using primary or
 secondary wet scrubbing.

 In many facilities (Vertical Stud Soderberg cells and side worked
 prebaked  cells),  potline  hooding  does  not  provide  adequate
 control  of  emission  from potline  cells,  and  pollutants  are
 released  into  the  potroom.   In the VSS configuration  of  the
 Soderberg process,  paste addition and pin adjustment occur above
 the  cell  and complete hooding is not possible.   As  a  result,
 facilities  with  the  VSS configuration  typically  use  potroom
 scrubbing  to  control the release of pollutants from  the  cell.
 Potroom air pollution control devices available are  limited,  by
 cost,  to wet scrubbers.   The applicable dry systems,  fluidized
 bed  alumina and injected alumina,  have not been cost  effective
 because  of the large volumes of air which must be treated.    All
 eight plants with secondary or potroom emission control in  EPA's
 data base use wet systems.

 It is reported lithium carbonate may be added to the electrolytic
 cells  to reduce power consumptions and increase production.    By
 adding lithium to the electrolytic cell,  physical properties  of
 the batch such as melting point, electrical conductivity,  and the
 density of the electrolyte are controlled.   An added benefit, and
 more relevant to this document, is that lithium reduces  fluoride
 emissions.

 Dry  potline  scrubbing  is reported to  be  detrimental   to   the
 manufacture^ certain high purity alloys.    Normally 100  percent
 of^the potline feed has been used  as scrubbing material; however,
 using  aluminum  in this manner tends to  concentrate  impurities
 such  as   iron  and   silicon  in  the  electrolytic   cell.    This
 precludes   use  of recycled alumina  as  a raw material to   produce
 these  alloys.    It is  possible,   however,   to  manufacture   high
 purity alloys  in  cells using  dry  scrubbers  if only  a  relatively
 small  percentage  (not  greater  than  approximately  20  percent)   of
 the   production  capacity is dedicated to the manufacture of these
 alloys.   Fresh  alumina is used to manufacture the alloys  and the
 alumina used  for scrubbing is used as feed  in  other cells.

 Wet   scrubbers are also used to control  sulfur  emissions from the
 potline.   These scrubbers differ from  those wet systems used  to
 control  fluoride  in  that  an alkali  solution  (normally sodium)  is
 used   for  scrubbing.    Use  of  alkali  scrubbers   follows   dry
 scrubbing  systems where particulate,   fluoride,  and organic  air
 pollutants  are  removed.   In  1984,  there were two  known   U.S.
 plants operating sodium scrubbers on  potline emissions to control
 sulfur oxides.

 Aluminum Fluxing and Degassing

 The  molten aluminum collected  in the bottom of the  electrolytic
 pots  is tapped and conveyed to holding furnaces  for  subsequent
 refining  and alloying.   Refining consists of fluxing to  remove
 impurities _and degassing to reduce entrapped hydrogen gas in the
molten aluminum.   Oftentimes fluxing and degassing are performed
                               630

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             PRIMARY ALUMINUM SUBCATEGORY   SECT - III
in the holding furnace prior to casting.   Degassing is performed
by injecting chlorine,  nitrogen,  argon,  helium and mixtures of
chlorine  and  inert gases into the  molten  aluminum.   Hydrogen
desorbs  into  the chlorine bubble due to  the  partial  pressure
difference  between the elements.   The addition of a gas to  the
melt  also mixes the aluminum to assure that all materials  added
concurrently  for  alloying are distributed evenly in the  molten
aluminum.

Besides  hydrogen,  other impurities that affect product  quality
are oxides of aluminum and magnesium,  and trace elements such as
sodium, calcium, and lithium.  Chlorine gas reacts with the trace
elements to form insoluble salt particles.   These salt particles
and the metal oxide impurities rise to the surface of the  molten
bath   through  specific  gravity  differences   and   flotation,
respectively.   The  impurities collected at the surface  of  the
molten  metal,  commonly referred to as dross,  are  skimmed  and
removed from the furnace.

Solid fluxes,  such as hexachloroethane,  aluminum chloride,  and
anhydrous  magnesium  chloride,  may be used instead  of  gaseous
fluxing.   These  fluxes are added to the surface of  the  molten
metal  and stirred in to obtain proper distribution and  contact.
It  is reported,  however,  solid fluxes are difficult to use and
generally  less efficient than gaseous fluxes.  Only one  primary
aluminum facility reported using solid fluxes.

Two  inherent  problems with furnace fluxing  and  degassing  are
corrosion and air pollution.   Emissions from the furnace consist
of  unreacted  chlorine  and  aluminum  chloride  gas.   Aluminum
chloride hydrolyzes in the stack and atmosphere to form acid mist
and  aluminum oxide fumes.  Fumes released by  furnace  degassing
and fluxing are treated by wet scrubbers at three plants.

There  are two refining procedures currently available which,  by
the  nature  of  their  operation,  reduce  chlorine  fumes  from
refining  operations and thus the need for air pollution  control
devices.  Chlorine fumes are reduced through the use of alternate
in-line  fluxing  and filtering techniques and with  the  MRL-P28
process  by containing the chlorine under a layer of molten  salt
and the subsequent formation of magnesium chloride.

Alternate  in-line fluxing and filtering is performed outside  of
the holding furnace just prior to casting.  There are three basic
in-line  fluxing and filtering techniques:   1)  flotation,    2)
impingement,  and 3) counter flow impingement.  Flotation in-line
fluxing is very similar to furnace degassing and fluxing methods.
A   mixture   of   gases,    including   chlorine,   is   bubbled
countercurrently  through the molten metal to remove  impurities.
Gas  is  distributed to the molten metal with  a  rotating  vane,
yielding better bubble distribution, and therefore better removal
efficiency  and  lower chlorine demands because a  stoichiometric
amount  of gas can be used.   In this way,  subsequent fuming  is
reduced because less chlorine is required.
                                631

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              PRIMARY ALUMINUM  SUBCATEGORY
SECT - III
 The  second in-line fluxing  technique  listed,  impingement,  is
 actually a^filtering technique.  A ceramic or fiberglass media is
 used  to filter the molten aluminum just prior to  casting.   In-
 line  filters  are reported to remove metal oxides so  that  only
 enough  chlorine  need  be  added to remove  hydrogen  and  trace
 metals.   Once  again,  fuming problems are reduced because  less
 chlorine  is  required.   Oftentimes this technology is  used  in
 conjunction with furnace fluxing.   Counter flow impingement  in-
 line  fluxing is a combination of the first two methods.   Gas is
 distributed  to the molten aluminum through the filter media  and
 then allowed to bubble up through the molten aluminum.

 In the MRL-P28 method of degassing, 97 percent nitrogen and three
 percent  Freon  12 is used.  A molten salt cover,  consisting  of
 sodium^chloride and potassium chloride or magnesium chloride  and
 potassium  chloride  is used to supress fuming.   It  is  reported
 this technology is technically equivalent to chlorine fluxing and
 reduces  stack  emissions  by a factor of  20  when  compared  to
 chlorine.

 Casting

 Casting is  the final step at most aluminum reduction plants.   Pig
 and  sow casting,   direct chill casting,   continuous rod casting,
 and  shot casting  are  the most  common methods of  casting used  in
 the primary aluminum subcategory.

 Vertical direct   chill casting is   characterized  by  continuous
 solidification of  the metal while it  is being poured.   The  length
 of an ingot  or billet cast  using  this  method  is determined  by the
 vertical distance   it   is  allowed  to  drop rather  than  by  mold
 dimensions.    Molten aluminum is  tapped from  the  smelting furnace
 and  flows   through  a  distributor  channel  into a  shallow  mold.
 Noncontact   cooling water circulates within   this  mold,  causing
 solidification of the aluminum.   The base  of  the  mold  is  attached
 to a  hydraulic cylinder which is  gradually  lowered   as  pouring
 continues.   As  the solidified aluminum leaves the mold,   it  is
 sprayed  with  contact cooling water to reduce  the temperature  of
 the  forming ingot or billet.   The cylinder  continues  to descend
 into a tank of water,   causing  further cooling of aluminum  as  it
 is immersed.   When the cylinder  has reached  its  lowest position,
 pouring  stops  and  the  ingot is  lifted  from  the  pit.   The
 hydraulic  cylinder  is  then raised and positioned  for  another
 casting  cycle.

 Horizontal direct chill casting is performed in much the  same way
 as  vertical direct chill casting.  The primary difference is that
 the  cast  aluminum is conveyed from the mold in  the  horizontal
 direction  rather than vertically.   Twenty-six primary  aluminum
 plants reported using direct chill casting.

 In continuous rod casting, a ring mold is fitted into the edge of
 a  rotating casting wheel.   Molten aluminum is then poured  into
 the mold and cools as the mold assembly rotates.   After the wheel
has  rotated  about  160 degrees,   the pliable  aluminum  bar  is
                               632

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             PRIMARY ALUMINUM SUBCATEGORY   SECT - III
released.   Immediately following release from casting the rod is
transported on conveyers to a rolling mill where the diameter  of
the  rod is reduced.  Thus it can be seen continuous rod  casting
is  generally  associated with aluminum forming.   Three  primary
aluminum  plants  reported using continuous rod casting  to  cast
molten aluminum extracted from the pots.

Stationary casting is used to cast pigs and sows.  In this method
of  casting,  the  molds are stationary and the  contact  cooling
water  generally  evaporates if it is used.   Eight  plants  with
stationary casting were identified.

One plant reported pebble casting which appears to be similar  to
shot casting.  Generally, aluminum shot is used as a deoxidant in
the  steel  industry.   Molten metal is poured into  a  vibrating
feeder,  where  droplets  of  molten  metal  are  formed  through
perforated openings.   The droplets are cooled in a quench  tank.
Water  is  generally  recycled,  and periodic sludge  removal  is
required.

Anode Paste Plant

Fabrication  of prebaked and Soderberg anodes takes place in  the
anode  paste plant where coal tar pitch and ground petroleum coke
are  blended together to form paste.   During  electrolysis,  the
prebaked anode is gradually consumed and becomes too short to  be
effective.   The  resulting  anode "butts," as they are  commonly
referred to, are recycled for use in the paste plant.  Operations
included in the paste plant are crushing,  screening,  calcining,
grinding,  and mixing.   The paste is then formed into briquettes
(for  use in Soderberg cells) or into green prebake  anodes.   At
this stage, briquettes and green anodes are essentially the same,
where   the  principal  difference  between  the  two  is   size.
Briquettes  are formed through an extrusion process in which  the
paste is forced through a die and then chopped into small  pieces
(briquettes) using a dicer.   Green anodes, which are much larger
than  briquettes,  are  formed  by pressing paste  Into  a  mold.
Vibration may also be used.  After forming, cooling water is used
to quench the briquettes or anodes to facilitate handling.  There
are  eleven  plants that report using anode or briquette  cooling
water.

Paste plant air pollution control usually consists of dry removal
of dust, although four plants use wet scrubbers.  There are eight
plants using dry air pollution control devices; however, only one
of  these  is used to control emissions from the  paste  blending
area.   Emissions  from  the  paste blending  area  contain  high
loadings  of  organics  and  are  normally  controlled  with  wet
scrubbers.

Carbon liners for the cell bottom are normally manufactured  off-
site.   However,  the  carbon  liner is sealed into the  cell  by
ramming paste into the cracks and seams of the liner.  Two plants
reported  using  wet scrubbers to control  emissions  during  the
blending of cathode paste.
                               633

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              PRIMARY ALUMINUM SUBCATEGORY   SECT - III
 Anode Bake Plant

 Anodes used in prebake potline cells are baked prior to their use
 in the potline.  Two basic furnaces are used to bake anodes: ring
 furnaces  and  tunnel  kilns.   The  ring  furnace  consists   of
 compartmentalized,  sunken,  brick baking pits  with  surrounding
 interconnecting  flues.  Green anodes are packed into  the  pits,
 with  a blanket of coke or anthracite filling the  space  between
 the  anode  blocks and the walls of the pits.  A 10  to  12  inch
 blanket  of  calcined petroleum coke fills the top  of  each  pit
 above  the  top layer of anodes.  The blanket  helps  to  prevent
 oxidation of the carbon anodes.

 Each pit is baked for a period of about 40 to 48 hours.  The flue
 system  of the furnace is arranged so that hot gas from the  pits
 being  baked  is  drawn  through the  next  section  of  pits  to
 gradually preheat the next batch of anodes before they are baked.
 Air  for  combustion  is drawn through  the  sections  previously
 baked,   cooling them down.  The anodes are baked at approximately
 1,200 C,  and_  the  cycle of placing  green  anodes,   preheating,
 baking,   cooling, and removal is approximately 28 days.   Roughly
 40  percent of the anode is volatilized during the baking cycle.

 Baking  of  sections  proceeds down one side of  the   rectangular
 furnace   building  and  back up the other  in  a  "ring"  pattern.
 Proceeding around the building,  the pattern of sections  cooling
 down,  sections  being  baked,  sections heating  up,   and  empty
 sections is repeated several times.

 Ring  furnaces use outside flues under draft,   and since the  flue
 walls  are  of   dry-type construction,   most   volatile   materials
 released  from   the anodes during the baking   cycle  (principally
 hydrocarbons   from  the  pitch  binder)   are  drawn,    with  the
 combustion products of the firing,  into the  flue gases  where they
 are burned at about 1300°C.

 Gaseous  emissions are  composed primarily of  fluoride  (present  due
 to  the   recycle   of   anode  butts)   and hydrocarbons   which  are
 controlled  through either wet scrubbers or dry   scrubbers   using
 alumina.   Five  plants  reported using  wet scrubbers  to control  air
 pollution, while  12 plants utilize dry  systems.

 The  baked anodes  are  stripped from  the  furnace pits by means  of
 an  overhead  crane  on  which  pneumatic  systems  for  loading  and
 removing  the  coke  pit  packing  may also  be mounted.   The  packing
may  subsequently  become part  of other green  anodes in  the  carbon
plant.

Ring furnaces can  be further subdivided  into  open and closed  top
furnaces.   A   closed  top furnace   is covered  with  a  movable
refractory arch lid.  An open  top furnace is  characterized by the
absence of the  refractory  lid.   Removal of the lid from a closed
top  furnace interrupts the flow path,  drawing the volatiles  up
through  the packing material  and directly into the  flue.   This
                               634

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             PRIMARY ALUMINUM SUBCATEGORY   SECT - III
method  of  operation  increases flue  life  and  decreases  fuel
consumption  because less air is required.  It is  reported  that
about  one-third  less  gases are processed  in  the  closed  top
furnace.

A second type of furnace, the tunnel kiln, has been developed for
baking anodes.   The kiln is an indirect-fired chamber in which a
controlled  atmosphere is maintained to prevent oxidation of  the
carbon  anodes.   Green  anode blocks are loaded  on  transporter
units that enter the kiln through an air lock,  pass successively
through a preheating zone, a baking zone, and a cooling zone, and
leave the kiln through a second air lock.  The refractory beds of
the  cars are sealed mechanically to the kiln walls to  form  the
muffle chamber,  and yet permit movement of the units through the
kiln.

The  muffle chamber is externally heated by combustion gases  and
the  products of combustion are discharged through an independent
stack  system.   Effluent  gases from the baking  anodes  may  be
introduced  into the fire box so as to recover the fuel value  of
hydrocarbons  and reduce the quantity of unburned hydrocarbon  to
approximately 1 percent of that coming from a ring furnace.

Although  the tunnel kiln presents mechanical problems in  design
and  operation,  it  is  reported  to  have  several  appreciable
ana  opei:atJ.
-------
              PRIMARY ALUMINUM  SUBCATEGORY   SECT -  III


 potliners are ground in a ball mill and then leached with caustic
 to  solubilize fluoride.  Undigested cathode material is separated
 from  the leachate using sedimentation and then sent to  lagoons.
 Sodium  aluminate  (NaAK>2)  is  then added to  the  leachate  to
 initiate  the  precipitation of cryolite (Na3AlF6) and  a  second
 solid-liquid  separation is performed to recover cryolite,  which
 can  be  reused in the electrolytic cell.  Lime is added  to  the
 supernatant  to precipitate calcium fluoride and a  third  solid-
 liquid  separation  is performed.  The resulting  supernatant  is
 then _ routed  back  to  the front of the  process  and  used  for
 leaching.   Blowdown from the system varies from plant to  plant,
 but  it  is universally used as potline scrubber  liquor  make-up
 when wet potline scrubbers are used.  It is also common to  route
 potline scrubber liquor through the cathode reprocessing circuit.
 In  this way, fluoride concentrations of the scrubber liquor  are
 controlled and recycle is possible.


 PROCESS WASTEWATER SOURCES

 The principal wastewater sources in the primary aluminum
 subcategory are:
      1,
      2,
      4,
      5.
      6.
      7.
      8.
      8.
      9.
     10.
     11.
     12.
Anode and cathode paste plant wet air pollution control,
Anode bake plant wet air pollution control,
Cathode reprocessing,
Anode and briquette contact cooling,
Potline wet air pollution control,
Potline SO2 wet air pollution control,
Potroom wet air pollution control,
Degassing wet air pollution control,
Pot repair and pot soaking,
Direct chill casting contact cooling,
Continuous rod casting contact cooling, and
Stationary and shot casting contact cooling.
OTHER WASTEWATER  SOURCES

Other  wastewater streams may be associated with  the  manufacture
of  primary  aluminum, or found at primary  aluminum  facilities.
These  wastewater streams may include coke plant  contact  cooling
water,  courtyard and  rooftop spray water,  paste  bucket  wash
water,  maintenance  and cleanup water,  stormwater  runoff,  and
spent  potliner leachate.  With the exception of  spent  potliner
leachate,  these   waste streams are not considered as a  part  of
this  rulemaking.   EPA  believes that the  flows  and  pollutant
loadings  associated  with these waste streams  are  either  "too
insignificant  to  warrant  a discharge allowance"  or  are  best
handled  by  the  appropriate permit authority on  a  case-by-case
basis under authority of Section 402 of the Clean Water Act.

While  EPA believes that spent potliner leachate is best  handled
by the appropriate permit authority on a case-by-case basis,  EPA
has provided guidance to permit writers on the issue of  leachate
treatment  performance values (.See Section X of this document and
                               636

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             PRIMARY ALUMINUM SUBCATEGORY
SECT - III
52 FR 25554).   That guidance states that spent potliner leachate
mayreceive  the  treatment  performance  values  developed  for
cathode  reprocessing or potline scrubber liquor commingled  with
cathode reprocessing wastewaters provided that the permit  writer
determines, on a case-by-case basis, that the wastewater matrices
of   cathode   reprocessing  and  spent  potliner  leachate   are
comparable.   Also,  the  spent  potliner  leachate  may  not  be
commingled  with  process or nonprocess  wastewaters  other  than
cathode   reprocessing  or  potline  wet  air  pollution  control
operated  in  conjunction  with  cathode   reprocessing.    Spent
potliner  leachate  resulting from atmospheric  precipitation  is
considered  to be a site-specific,  non-scope waste stream by the
Agency.   As such, specific limitations are not provided for this
waste stream in 40 CFR Part 421, 88421.23, 421.24, and 421.26.

AGE, PRODUCTION, AND PROCESS PROFILE

Figure  III-2  (page 642) shows the location of  the  31  primary
aluminum  reduction  plants  operating  in  the  United   States.
Because considerable amounts of electrical energy are required to
produce aluminum,  most primary aluminum plants are located  near
sources of abundant and inexpensive hydroelectric power, such  as
the Pacific Northwest and the Tennessee River Valley.

Of  the 31 reduction plants listed in Table III-l, (page 638)  22
plants (70 percent) were built in the last 33 years.  The average
plant  age  is between 20 and 30 years.  The data  summarized  in
Table  III-2  (page 639) indicate that 27 of the  31  plants  (85
percent)  produce less than 200,000 tons per year  each.   Median
production is in the 100,000 to 150,000 tons per year range.

Table III-3 (page 640) provides a summary of the number of plants
generating  wastewater for the waste streams associated with  the
various processes and the number of plants with the process.
                               637

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PRIMARY ALUMINUM SUBCATEGORY   SECT - III

















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        PRIMARY ALUMINUM SUBCATEGORY   SECT - III
                      Table III-2

PRODUCTION RANGES FOR THE PRIMARY ALUMINUM SUBCATEGORY
     Production Ranges
    for 1976 (tons/year)

          0 - 50000

      50001 - 100000

     100001 - 150000

     150001 - 200000

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     in Survey
No. of Plants

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    31
                          639

-------
              PRIMARY ALUMINUM SUBCATEGORY    SECT  -  III
                            Table  III-3
  SUMMARY OP SUBCATEGORY PROCESSES  AND  ASSOCIATED WASTE  STREAMS
                                      Number of
                                     Plants with
                                       Process

                                         31

                                         28
                                          2
                                          8

                                         29

                                         26
          Process

Electrolytic Reduction

  Potline Air Pollution Control
  Potline SC-2 Air Pollution Control
  Potroom Air Pollution Control

Anode Paste Plant

  Anode Paste Plant Air Pollution
     Control

Anode Bake Plant                        20

  Anode Bake Plant Wet Air Pollution    17
      Control

Anode Contract Cooling and Briquette    11
      Quenching

Cathode Reprocessing                     4

Pot Repair and Pot Soaking              31

Refining                                13

  Degassing Air Pollution Control        6

Casting

  Direct Chill Casting                  26
  Continuous Rod Casting                 3
  Stationary Casting                     8
  Shot Casting                           1
Number of Plants
  Generating
  Wastewater
     9
     2
     8
                                                      11
                                                       4

                                                       5*
                                                      26
                                                       3
                                                       0
                                                       1
* Number of Plants known to discharge pot soaking and pot  repair
wastewater.
                               640

-------
     PRIMARY ALUMINUM SUBCATEGORY
                               SECT -  III
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PRIMARY ALUMINUM SUBCATEGORY
SECT  -  III
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               PRIMARY ALUMINUM SUBCATEGORY   SECT - IV



                            SECTION IV

                         SUBCATEGORIZATION
This   section  summarizes  the  factors  considered  during  the
designation  of the primary aluminum subcategory and its  related
subdivisions.   Primary  aluminum  was  considered  as  a  single
subcategory during the previous 1974 rulemaking.
FACTORS   CONSIDERED   IN  SUBDIVIDING   THE   PRIMARY
SUBCATEGORY
ALUMINUM
The  factors  listed  for  general  subcategorization  were  each
evaluated N when  considering subdivision of the primary  aluminum
subcategory.  In the discussion that follows, the factors will be
described as they pertain to this particular subcategory.

The  rationale  for  considering  segmentation  of  the   primary
aluminum subcategory is based primarily on the production process
used.   Within this subcategory, a number of different operations
are  performed,  which  may  or  may  not have  a  water  use  or
discharge,  and  which may require the establishment of  separate
effluent  limitations  and  standards.   While  primary  aluminum
smelting  is  still  considered  a  single  subcategory,  a  more
thorough examination of the production processes,  water use  and
discharge   practices,   and   pollutant  generation  rates   has
illustrated  the  need for limitations and standards based  on  a
specific set of waste streams.  Limitations and standards will be
based on specific flow allowances for the following subdivisions:

      1.  Anode and cathode paste plant wet air pollution
          control,
      2.  Anode bake plant wet air pollution control,
      3.  Cathode reprocessing,
      4.  Anode and briquette contact cooling,
      5.  Potline, wet air pollution control,
      6.  Potline SO2 wet air pollution control,
      7.  Potroom wet air pollution control,
      8.  Degassing wet air pollution control,
      9.  Pot repair and pot soaking,
     10.  Direct chill casting contact cooling,
     11.  Continuous rod casting contact cooling, and
     12.  Stationary and shot casting contact cooling.

OTHER FACTORS

A number of other factors considered in this evaluation and  were
shown  to  be  an inappropriate bases for  further  segmentation.
These are discussed briefly below.

Type of Anode

As  described in Section III,  there are two anode types used  by


                               643

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                PRIMARY ALUMINUM SUBCATEGORY
SECT - IV
 the primary  aluminum subcategory;   prebaked  and   Soderberg.    The
 type  of   anode   used determines  the  wastewater  source   in   which
 particular  toxic  organic  pollutants appear.    In   plants   using
 prebaked  anodes,   toxic  organic pollutants have  been observed   in
 wastewater from wet air  pollution  control devices associated with
 the anode bake plant and in plants using Soderberg anodes,   toxic
 organics   have  been  observed  in potline and   potroom   wet  air
 pollution control devices.   However,   the concentrations of  the
 toxic   organics   observed  in  both wastewater   sources   were   at
 similar levels,   requiring  similar treatment  (refer  to Sections V
 and VII).  Accordingly,  subdivision of the category  by anode type
 was rejected.

 Plant  Size

 A   review of  the 31 aluminum reduction plants   showed   that   11
 plants have capacities  of  less than  90,000 metric tons   (100,000
 short   tons) per  year,   16  plants  have capacities between 90,000
 and 180,000 metric  tons  (100,000 and 200,000   short   tons  per
 year),  and  three  plants  have capacities greater   than 180,000
 metric tons (200,000 short tons)  per  year.   No factors relating
 to   this   distribution of plant size  and pertaining   to   a   given
 plant's   ability  to achieve  effluent  limitations  have  been
 identified.

 Plant  Age

 Primary aluminum  smelting is a relatively new industry based on a
 single  process.    Therefore, the oldest plants built  in  the  early
 1940's  are  electrochemically equivalent to those  built  today;
 however,   numerous   modifications  have  been   made  in process
 operation  which  have resulted in  greater  production  efficiency
 and reduced air  pollutant  emissions.   As a result,  neither  the
 concentration of  constituents in wastewater nor  the capability  to
 meet   the  limitations is  related to plant age.    Because of   the
 general    uniformity   of  aluminum   process    technology,    the
 application  of   most environmental control methods  and systems
 that  have been developed is dependent  on factors other  than  age
 (i.e.,  for  the  Hall  process,  the most recently developed  unit
 operations   are used,  and  these can be retrofitted independently
 of  plant age).

 Product

 Primary  aluminum smelters  produce aluminum metal  and  various
 aluminum  alloys.    Some  plants carry  out an additional   refining
 step  to produce  higher purity aluminum,  and a  few  plants  also
 carry  out rolling and wire-drawing operations.   The fabrication
 operations rolling,   drawing,  forging, and extrusion are covered
 under a separate  point source category.

 PRODUCTION NORMALIZING PARAMETERS

As discussed previously,  the effluent limitations and   standards
 developed  in  this document establish mass  limitations  on  the
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               PRIMARY ALUMINUM SUBCATEGORY   SECT - IV
discharge  of  specific  pollutant parameters.    To  allow  these
limitations  and guidelines to be applied to plants with  various
production  capacities,  the mass of pollutant  discharged must be
related  to a unit of production.   This factor is known  as  the
production normalizing parameter (PNP)«   In general,  the amount
of  aluminum produced by the respective manufacturing process  is
used as the PNP.   This is based on the principle that the amount
of water generated is proportional to the amount of product made.
The  PNP's  for the 12 subdivisions are displayed in  Table  VI-1
(page 659). Other PNPs were considered for certain  subdivisions;
however, they were rejected.  They are discussed below.

ANODE AND CATHODE PASTE PLANT WET AIR POLLUTION CONTROL

The   production   normalizing   parameter  selected   for   this
segment  is the actual paste production,  as metric  tons  (short
tons)  of paste.   Overall aluminum reduction capacity,  although
considered as a parameter,  was rejected;  since some plants sell
paste  and anodes to other plants,  it is difficult to  ascertain
which  plants  were  selling and which  plants  were  purchasing.
Records are available,  however, that detail paste plant capacity
and  production  levels.   Capacity,  rather  than  actual  paste
production,  was  considered  for use because the water  use  and
discharge  rates  reported  by the plants were for  a  year  when
capacity  utilization  in the primary  aluminum  subcategory  was
abnormally low.  When analytical samples were taken, however, the
pollutant   concentration  calculations  were  based  on   actual
measured  flows and production rates.   In order to be consistent
when determining pollutant loadings,  the actual paste production
was  chosen  as the production  normalizing  parameter.   Use  of
actual  paste  production also eliminates the need for plants  to
reduce  water  flow during years in which  actual  production  is
greater than design capacity.

CATHODE REPROCESSING

The   production   normalizing   parameter  proposed   for   this
subdivision was the amount of aluminum produced from electrolytic
reduction.   The  Agency has learned since proposal that  certain
primary aluminum plants may process cathodes from other plants as
a  hazardous  waste  treatment  operation.    Consequently,   the
aluminum produced from electrolytic reduction is an inappropriate
production  normalizing parameter.   A more  suitable  production
normalizing  parameter is the amount of cryolite recovered during
cathode reprocessing.   In  this way, cathode reprocessing becomes
independent of  the reduction process so that cathodes  from  other
plants may be brought  to one site  for processing.

POTLINE, POTLINE SO2/  AND POTROOM  WET AIR POLLUTION CONTROL

Most  plants  use wet  or dry scrubbing over an  entire  potline  or
potroom   (i.e.,  the   off-gases  are  collected,  and   centralized
scrubbers  are  used to control   the   emissions).   Occasionally,
though,  a  plant  may use wet  scrubbers on only  one of   their
potlines.    Therefore,    the   production   normalizing parameter
                                645

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               PRIMARY ALUMINUM SUBCATEGORY   SECT - IV


selected  for  these  subdivisions  is  the  amount  of  aluminum
produced from electrolytic reduction.   If wet scrubbers are only
used on a particular potline,  the amount of aluminum produced is
based on the electrolytic reduction in that potline.  Although it
should_be noted that actual aluminum production from, electrolytic
reduction can exceed rated capacity, this is generally achievable
only with a loss in current efficiency.   Discussions with  plant
personnel  indicated  that capacity might be a  more  appropriate
measure   than  actual  aluminum  production  from   electrolytic
reduction  because  when the potline is operating,  water use  is
relatively  constant  (i.e.,   water  use  is  not  adjusted  for
production rates).  When an entire potline is shut down, then the
scrubbers are shut down as well.   Consistency in the application
of  sampling  data,  however,  necessitated the use  of  aluminum
production   from   electrolytic  reduction  as  the   production
normalizing  parameter.    This will ensure that  higher  capacity
utilization  will  not  reduce  the  production  normalized  flow
allowance for this operation.
                              646

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               PRIMARY ALUMINUM SUBCATEGORY
                                         SECT - IV
                           TABLE IV-1

                PRODUCTION NORMALIZING PARAMETERS
 8.
10,
11,
12,
          Subdivision

     Anode and cathode paste plant
      wet air pollution control

     Anode bake plant wet air
      pollution control

     Anode and briquette contact
      cooling

     Cathode reprocessing
Potline wet air pollution
 control

Potline SO2 wet air
 pollution control

Potroom wet air pollution
 control

Degassing wet air pollution
 control

Pot repair and pot soaking
Direct chill casting contact
 cooling

Continuous rod casting
 contact cooling

Stationary or shot casting
 contact cooling
                                      PNP

                                kkg of paste produced


                                kkg of anodes baked
kkg of anodes or briquettes
 cast

kkg of cryolite produced
 from cathode reprocessing

kkg of aluminum produced
 from electrolytic reduction

 kkg of aluminum produced
 from electrolytic reduction

kkg of aluminum produced
 from electrolytic reduction

kkg of aluminum degassed
kkg of aluminum produced
 from electrolytic reduction

kkg of aluminum product
 from direct chill casting

kkg of aluminum product
 from rod casting

kkg of aluminum product
 from stationary or shot
 casting
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PRIMARY ALUMINUM SUBCATEGORY   SECT - IV
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                PRIMARY ALUMINUM  SUBCATEGORY    SECT  - V




                             SECTION V

             WATER USE AND WASTEWATER CHARACTERISTICS
 This   section  describes  the  characteristics   of   wastewater
 associated  with  the primary aluminum subcategory.   Data used  to
 quantify   wastewater  flow  and  pollutant  concentrations   are
 presented,   summarized,  and  discussed.   The  contribution   of
 specific production processes to the overall wastewater discharge
 from  primary  aluminum plants is identified  whenever  possible.
 This  information  was used primarily to identify principal sources
 of wastewater in  the category and to determine if pollutants were
 present  in  treatable  concentrations.   Treatment   performance
 concentrations were developed from different data bases.

 Three principal data sources were used in the development of  the
 effluent  limitations and standards for this  subcategory:   data
 collection portfolios (dcp),  field sampling results and comments
 and   associated   specific  data   requests.   Data   collection
 portfolios,  completed  for each of the primary aluminum  plants,
 contain  information  regarding wastewater flows  and  production
 levels.

 In  order  to  quantify  the  pollutant  discharge  from  primary
 aluminum  plants,   a  field  sampling  program  was   conducted.
 Wastewater  samples were collected in two phases:   screening and
 verification.   The first phase, screen sampling, was to identify
 which  toxic  pollutants  were present in  the  wastewaters  from
 production  of  the  various  metals.    Screening  samples  were
 analyzed for 125  of the 126 toxic pollutants and other pollutants
 deemed  appropriate.    Because the analytical standard for  TCDD
 was  judged to be too hazardous to be made  generally  available,
 samples  were  never analyzed for this pollutant.   There  is   no
 reason  to expect that TCDD would be present in aluminum smelting
 wastewater.    A  total  of 10 plants were  selected  for  screen
 sampling  in  the nonferrous metals  manufacturing  category.   A
 complete  list of the pollutants considered and a summary of  the
 techniques used in sampling and laboratory analyses are  included
 in  Section V of  the General Development Document.   In  general,
 the samples were analyzed for three classes of pollutants:  toxic
 organic   pollutants,  toxic  metal  pollutants,    and   criteria
 pollutants (which includes both conventional and  nonconventional
 pollutants).

As  described  in  Section IV of  this  supplement,   the  primary
 aluminum  subcategory has been further segmented into 12 building
 blocks,   so  that  the  promulgated  regulation  contains   mass
discharge  limitations and standards for 12 process   wastewaters.
Differences  in  the wastewater characteristics  associated  with
 these  building  blocks  are to be expected.    For  this  reason,
wastewater  streams corresponding to each segment  are  addressed
separately in the discussions that follow.
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                PRIMARY ALUMINUM SUBCATEGORY   SECT - V
 WASTEWATER SOURCES , DISCHARGE RATES/ AND CHARACTERISTICS

 The  wastewater data presented in this section were evaluated  in
 light  of  production  process information compiled  during  this
 study.   As a result,  it was possible to identify the  principal
 wastewater  sources in the primary aluminum  subcategory.    These
 include:

       1.  Anode and cathode paste plant wet air pollution
           control,
       2.  Anode bake plant wet air pollution control,
       3.  Anode and briquette contact cooling,
       4.  Cathode reprocessing,
       5.  Potline wet air pollution control,
       6.  Potline SC>2 wet air pollution control,
       7.  Potroom wet air pollution control,
       8.  Refining and degassing wet air pollution control,
       9.  Pot repair and pot soaking,
      10.  Direct chill casting contact cooling  water,
      11.  Continuous rod casting contact cooling water,  and
      12.  Stationary and shot casting contact cooling  water.
                                                               ft
 Data   supplied  by  dcp  responses (and  special   requests)   were
 evaluated,   and two flow-to-production ratios were calculated for
 each  stream.    The two ratios, water use and wastewater  discharge
 flow,   are  differentiated by the flow value used in calculation.
 Water  use  is  defined as the volume of water or  other fluid  (e.g.,
 emulsions,   lubricants)   required for a given process  per mass of
 aluminum product and is therefore based on  the  sum of  recycle and
 make-up flows to a  given process.    Wastewater  flow  discharged
 after   pretreatment  or recycle  (if these are present)  is used in
 calculating   the production normalized  flow — the   volume   of
 wastewater  discharged from a given process to  further treatment,
 disposal,   or   discharge  per   mass   of    aluminum   produced.
 Differences between  the water use and wastewater flows associated
 with   a given  stream  result   from  recycle,  evaporation,  and
 carryover   on  the  product.   The  production  values  used   in
 calculation  correspond to the production normalizing  parameter,
 PNP,   assigned  to each stream,  as  outlined in Section  IV.   The
 production  normalized  flows were  compiled  and  statistically
 analyzed by stream type.   Where  appropriate, an attempt was   made
 to  identify  factors  that  could  account  for  variations  in  water
 use.   This  information is  summarized  in  this  section.  A  similar
 analysis of factors  affecting the  wastewater values is  presented
 in  Sections   X,  XI,  and XII  where  representative BAT,  BDT,  and
 pretreatment  discharge flows  are  selected for use  in  calculating
 the  effluent  limitations  and standards.  As an example,  potline
 air  scrubbing   waste  water  flow   is   related  to  the  potline
production.   As  such,  the discharge  rate is expressed in  liters
of  scrubber  wastewater   per metric  ton  of  potline  production
 (gallons of scrubber water per ton  of potline production) .

The  methods  used   in evaluation of wastewater  data  varied  as
dictated  by  the  intended  use of  the  results.   For  example,  in
Section VI  the wastewater  data from effluent samples are examined
                               650

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               PRIMARY ALUMINUM SUBCATEGORY   SECT - V


to   select  pollutants  for  consideration  in  regulating   the
category.

In order to quantify the concentrations of pollutants present  in
wastewater from primary aluminum plants,  wastewater samples were
collected  at  six  plants,   representing  22  percent  of   the
discharging  primary aluminum plants.   Diagrams  indicating  the
sampling sites and contributing production processes are shown in
Figures V-l to V-6 (pages 718 to 723).

The  raw  wastewater  sampling  data  for  the  primary  aluminum
subcategory are presented in Tables V-2, 4, 6, 8, 10, 13, 15, and
20 (pages 660,  663, 666, 669, 675, 679, 687, 693, respectively).
Miscellaneous  wastewater sampling data are presented in Table V-
21  (page 695).   Treated wastewater sampling data are  shown  in
Tables  V-22  through V-27 (pages 701 to 710).  The  stream  codes
displayed  in Tables V-12 through V-27 (pages 680 to 710) may  be
used  to  identify  the location of each of the  samples  on  the
process  flow diagrams in Figures V-l to V-6 (pages 718 to  723).
Where  no  data are listed for a specific day  of  sampling,  the
wastewater  samples  for the stream were not collected.   If  the
analysis  did  not   detect a pollutant in a  waste  stream,  the
pollutant was omitted from the table.

The  data tables include some samples measured at  concentrations
considered not quantifiable.   The base-neutral extractable, acid
extractable,  and volatile organics are generally considered  not
quantifiable  at concentrations equal to or less than 0.010 mg/1.
Below  this  concentration,  organic analytical results  are  not
quantitatively  accurate;  however,  the analyses are  useful  to
indicate  the presence of a particular pollutant.   The pesticide
fraction is considered nonquantifiable at concentrations equal to
or less than 0.005 mg/1.   Nonquantifiable results are designated
in the tables with an asterisk (double asterisk for pesticides).

These  detection limits shown on the data tables are not the same
in  all  cases  as  the  published  detection  limits  for  these
pollutants by the same analytical methods.   The detection limits
used  were  reported with the analytical data and hence  are  the
appropriate  limits  to  apply  to  the  data.   Detection  limit
variation  can  occur  as a result of  a  number  of  laboratory-
specific,   equipment-specific,   and   daily   operator-specific
factors.   These  factors  can include day-to-day differences  in
machine calibration,  variation in stock solutions, and variation
in operators.

The  statistical analysis of data includes some samples  measured
at concentrations considered not quantifiable.   Data reported as
an  asterisk  are considered as detected but  below  quantifiable
concentrations, and a value of zero is used for averaging.  Toxic
organic,  nonconventional,  and conventional data reported with  a
"less  than"  sign are considered as detected,  but  not  further
quantifiable.   A value of zero is also used for averaging.  If  a
pollutant  is  reported  as  not  detected,  it  is  excluded  in
calculating the average.  Finally, toxic metal values reported as
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                PRIMARY ALUMINUM  SUBCATEGORY
SECT - V
 less  than a  certain value were  considered as not detected,  and a
 value of zero  is used  in the calculation of  the  average.   For
 example,  three samples  reported as ND,  *, and 0.021 mg/1 have an
 average  value   of  0.010  mg/1.   The   averages  calculated  are
 presented with  the sampling data.   These values were not used in
 the selection of pollutant parameters.

 The   method  by which each sample was collected is  indicated  by
 number, as follows.

      1     one-time grab
      2     24-hour manual composite
      3     24-hour automatic composite
      4     48-hour manual composite
      5     48-hour automatic composite
      6     72-hour manual composite
      7     72-hour automatic composite

 In the dcps, plants were asked  to indicate whether or not any  of
 the   toxic   pollutants  were  believed to  be  present  in  their
 wastewater.   Responses for the toxic organic compounds  selected
 as    pollutant   parameters  and  toxic   metals   considered   for
 regulation   are summarized in Table V-28 (page  712)  for  those
 plants  responding to that portion of the dcp.  Although most  of
 the   plants  indicated that these compounds were believed  to  be
 absent, several did report that they believed specific  pollutant
 parameters were present in their wastewater.


 ANODE AND CATHODE PASTE PLANT WET AIR POLLUTION CONTROL

 Plants manufacturing Soderberg and prebaked anodes blend coal tar
 pitch and ground coke (metallurgical and petroleum) to form anode
 paste.   Plants  may also prepare cathode paste to seal the seams
 the   cathode to  prevent iron contamination.   These raw materials
 are crushed, screened, calcined, ground, and blended in the paste
 plant.   This   series of operations results in the  formation  of
 particulates, tars, oils, and hydrocarbons through degradation of
 the pitch and coke.   Four of the 29 facilities with paste plants
 report  the use  of wet scrubbers to control the emission of these
 pollutants while 22 report the use of dry air pollution  control.
 Anode  paste plant wet air pollution control discharge levels are
 in  liters/metric  ton (1/kkg)  (gal/ton) of  paste  produced,  as
 shown in Table V-l (page 659).

 Plants  using  wet  air  pollution control  on  the  paste  plant
 generally  do so to control fugitive hydrocarbon emissions.   The
 variation  in the production normalized flows shown in Table  V-l
may be a result  of the degree of hydrocarbon control required  in
 each plant.

Table  V-2 (page 660)  summarizes the field sampling data for  the
 toxic  and selected conventional and  nonconventional  pollutants
detected.   This  waste stream is characterized by the presence of
the  toxic  organics  acenaphthene,    naphthalene,   fluoranthene,
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               PRIMARY ALUMINUM SUBCATEGORY   SECT - V
benzo(a)anthracene,   chrysene,   phenanthene,  fluorene,  and pyrene
(all above 1 mg/1)  and the conventional pollutant, oil  and grease
(25 to 1,900 mg/1).    These specific pollutants are present as  a
result of the crushing, screening, and calcining of the pitch and
coke.

ANODE BAKE PLANT WET AIR POLLUTION CONTROL

Of  the 20 primary aluminum plants with anode bake  plants,  five
utilize  wet air pollution controls on anode bake furnaces.   The
water discharge rates for anode bake plant air pollution  control
are  shown in Table V-3 (page 662).   Suspended solids,  oil  and
grease,   sulfur   compounds   and   fuel   combustion   products
characterize  this  effluent  stream.    Fluorides  may  also  be
introduced in plants where recycle of anode "butts" is practiced.
The  toxic organic pollutants found in anode paste plant wet  air
pollution control wastewater are also present in anode bake plant
wet  air  pollution  control samples.   These  pollutants  evolve
during  the baking of green   anodes in the bake  plant,  and _as
such  are present in the wastewater.   Anode bake plant  sampling
data are presented in Table V-4 (page 663).

ANODE AND BRIQUETTE CONTACT COOLING

Eleven  plants  report the use of water for cooling green  anodes
and briquettes prior to their introduction into the  electrolytic
cell.   Three  of  the  11 plants use contact cooling  water  for
Soderberg  briquettes.   Water discharge rates for the 11  plants
reporting  the  anode  contact  cooling  wastewater  stream   are
presented  in  liters per metric  ton of anode cast in  Table  V-5
(page 665). This waste stream is  characterized by the presence of
many  of  the  toxic  organics discussed  above  but  at  reduced
concentrations (0.04 to 0.08 mg/1).   The raw wastewater data for
this stream are shown  in Table V-6  (page 666).

CATHODE REPROCESSING

The  electrolytic  pot is lined with a cathode manufactured  from
anthracite coal.  Upon the failure  of a cathode, the pot is taken
out of production, emptied, rinsed, and the liner is removed. The
cathode   is then transferred to cathode reprocessing where it  is
ground and leached with caustic to  solubilize fluoride.  Cryolite
is  precipitated  from the leachate by the  addition  of  sodium
aluminate.   (The operation is conducted to treat hazardous  waste
as  well  as   to recover cryolite).  The  water  discharge  rates
reported  for  cathode  reprocessing,  in liters per metric   ton  of
cryolite  recovered, are shown  in Table V-7  (page 668).    Due  to
the  raw  materials used to manufacture the cathode,   this  waste
stream   is  characterized  by   the  presence  of  toxic    organic
pollutants  (less than  0.05 mg/1).   Fluoride  (63  to 13,000  mg/1),
cyanide   (58   to  129  mg/1), and  total suspended  solids   (19  to
54,500  mg/1)  are also present.   The presence of  cyanide   results
from   the electrolytic  process  where high   temperatures  and   a
reducing  environment  induce the formation  of  cyanide from  carbon
•and  nitrogen.  The  raw wastewater  data are  shown  in  Table  V-8
                                653

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                PRIMARY ALUMINUM SUBCATEGORY   SECT - V
 (page 669).

 POTLINE WET AIR POLLUTION CONTROL

 For potline emissions,   the water use and discharge  in liters  per
 metric ton of aluminum from electrolytic reduction production  are
 shown in Table V-9 (page 674).    Flow rates  are  only based on  the
 production  of those potlines controlled by  a  wet  system.    Raw
 wastewater  characterization  data for potline wet air  pollution
 control,  as  shown in Table V-10,  (page 675) are  from  samples
 taken  at  three  primary aluminum plants.   Waste  streams  from
 potline wet scrubbers or wet electrostatic precipitators  contain
 suspended   solids,   fluorides  and  several  toxic  pollutants.
 Suspended  solids  result from dust associated with   alumina   and
 cryolite  addition to the electrolytic  cell.    Fluoride  results
 from the use of cryolite,  a fluoride salt in the  cell.    Organic
 pollutants  present  can be attributed to anode  oxidation.    In
 addition, toxic metal impurities  in the alumina  can  be introduced
 into this waste stream.   These  are introduced as part of the dust
 evolving from the anode.

 POTLINE SO2 WET AIR POLLUTION CONTROL

 Two ^plants  currently   use sodium scrubbers  to  control  sulfur
 dioxide emissions from  potlines.   In both instances  the  scrubbers
 follow  dry fluoride scrubbing  systems.    Although the Agency  has
 not  sampled  this  wastewater  source,   it will  contain  similar
 pollutants  as  potline  wet air pollution control,   but  at  much
 smaller  concentrations.    Dry  fluoride  scrubbing   systems   are
 reported to have efficiencies approaching 99.9 percent removal  of
 fluoride and 80 percent  of  organic  emissions.   Therefore,  this
 waste  stream is expected  to be  relatively pollutant  free,  with a
 pH   between 6  and 7.   Water  use  rates  on a production normalized
 basis  are presented in Table  V-ll  (page  679).

 POTROOM WET AIR POLLUTION CONTROL

 For  potroom emissions control devices,  the anode type, water use,
 and  water  discharge  rates,   in liters per metric  ton  of aluminum
 from electrolytic  reduction,  are  shown  in Table V-12  (page 680).
 Flow  rates  are   only based  on production  levels   of  potlines
 controlled  by  a  wet  system.   As can  be  seen in Table  V-13, (page
 681)   potroom   air pollution  control  wastewater  streams   contain
 pollutants   similar   to   those  associated with   the  potlines   at
 reduced   concentrations.    This  is   due  to the   fact   that  air
 circulated   through  potroom  scrubbing systems is  diluted  as   it
 passes   from the pots through the  air space above  the  potline   to
 the  scrubbing  system  in the roof.

 DEGASSING WET AIR POLLUTION CONTROL

Most aluminum  reduction plants  degas molten aluminum before cast-
 ing.   Degassing  is  usually   accomplished  by  bubbling  a  gas
 (chlorine,   nitrogen,  argon, or a combination of  these elements)
 through  the melt.  The reported water use and discharge rates for
                               654

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               PRIMARY ALUMINUM SUBCATEGORY   SECT - V
degassing wet air pollution control,  in liters per metric ton of
aluminum  degassed,  are  shown in Table V-14  (page  686).   Raw
wastewater  from  this  waste  stream  is  characterized  by  the
presence  of toxic metals at very low  concentrations.   The  raw
wastewater data are shown in Table V-15 (page 687).

POT REPAIR AND POT SOAKING

Periodically  electrolytic cells fail,  and the carbon  liner  or
cathode is removed.   Generally water is used to soften the liner
and  to  facilitate  removal.   Water dumped from the  cell  will
contain  cyanide  and fluorides similar to  cathode  reprocessing
wastewater.  Analytical data supplied by industry representatives
show  TSS  concentrations ranging from 10-400 mg/1  and  fluoride
ranging from 1,800-7,000 mg/1.  Cyanide was reported as 438'mg/1.
Data on water use for this process are limited.   Several  plants
were  contacted  through Section 308 authority after proposal  to
try  to quantify water usage.   Data were received from only  one
company,  indicating water usage rates of 710 1/kkg to 3.3  1/kkg
of  aluminum reduced.   Additional water use data were taken from
the dcp and comments on the draft development document.   Another
plant  visited  by the Agency was designed as  a  zero  discharge
system  through 100 percent reuse.   Conversations with  industry
personnel  indicate  this operation is normally a zero  discharge
operation  through continued reuse of the soaking  water.   Three
plants  are known to reuse 100 percent of their  pot  soaking-pot
repair  wastewater.   Water usage rates are presented in Table V-
16 (page 688).

CASTING CONTACT COOLING WATER

Contact cooling water may be used for casting.  The cooling water
is frequently recycled but may require a bleed stream  (blowdown)
to  dissipate  the buildup of dissolved solids.   There are  four
principal   types  of  casting  used  in  the  primary   aluminum
subcategory:  direct chill, stationary, shot, and continuous rod.
Twenty-six primary aluminum plants practice direct chill casting,
eight plants practice stationary casting,  one .has shot  casting,
and three plants have continuous rod casting operations.   In the
stationary  casting method,  molten aluminum is poured into  cast
iron molds and then generally allowed to air cool.  The Agency is
aware  of the use of spray quenching to quickly cool the  surface
of  the molten aluminum once it is cast into the molds;  however,
this  water evaporates on contact with the molten  aluminum.   As
such,  the Agency believes that there is no basis for a pollutant
discharge  allowance.   The  water use and  discharge  rates  for
direct  chill and continuous rod casting operations are shown  in
Tables  V-17 through V-19 (pages 689-692), in liters  per  metric
ton  of aluminum cast.  Organics, in the form of oil  and  grease
(and total phenolics (4-AAP)), may be found in these systems when
lubricants  are  applied.  The variety and quantity  of  organics
will  be dependent on the type of lubricant used.  Sampling  data
for a direct chill casting operation are presented in Table  V-20
(page 693).
                               655

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               PRIMARY ALUMINUM SUBCATEGORY
SECT - V
The data in the raw wastewater table show that,  when compared to
the plant intake water analyses,  over half of the raw wastewater
pollutants are nearly the same or only slightly higher (less than
one  order  of magnitude) than the intake  water.   Although  the
sampling  data  in  Table V-20 (page 693)  is  for  direct  chill
casting,  contact  cooling water from other types of casting will
have similar pollutant characteristics because the raw  material,
aluminum, is the same in all four operations.

PILOT SCALE WASTEWATER TREATMENT STUDY

Subsequent  to proposing amendments to the  effluent  limitations
and  standards for the primary aluminum subcategory,  the  Agency
received numerous comments from companies in the primary aluminum
subcategory  on the proposed mass limitations for  benzo(a)pyrene
and cyanide.  To respond to these comments, the Agency  conducted
bench  and  pilot-scale  tests on  potline  scrubber  liquor  and
cathode reprocessing wastewater to determine the effectiveness of
various  wastewater  treatment methods  in  removing  polynuclear
aromatic  hydrocarbons (PAH) and on the effectiveness of  cyanide
precipitation  in removing cyanide from cathode reprocessing  and
potroom wet air pollution control wastewater.  In the study,  the
effectiveness  of  lime and settle,  multimedia  filtration,  and
activated carbon were examined  using bench scale and pilot scale
equipment in a trailer mounted wastewater treatment facility at a
primary aluminum plant in the northwestern United States.

PAH Treatment

The  study  demonstrated  that  PAH  commonly  found  in  primary
aluminum  wastewaters  can  be  removed  using  lime  and  settle
technology  followed by multimedia filtration.   In  this  study,
benzo(a)pyrene  was removed to the quantification limit of  0.010
mg/1  by lime settle and filter technology.   It was demonstrated
that  activated  carbon will also reduce  benzo(a)pyrene  to  the
nominal  quantification limit of 0.010 mg/1.   Analytical results
of the study are presented in Tables V-29 through V-33 (pages 713
-717).

Data  obtained  from the pilot scale work were  used  to  develop
achievable  treatment  concentrations for the various  PAH  using
lime and settle;  lime,  settle,   and multimedia filtration;  and
lime,   settle,   multimedia  filtration,  and  activated  carbon
adsorption   treatment.    These   long-term  average   treatment
effectiveness  concentrations  were also  used  in  recalculating
pollutant removal estimates.

For the model treatment technology, lime, settle, and filter, the
Agency calculated values of 0.0337 mg/1 for the daily maximum and
0.0156  mg/1 for the average monthly maximum.   These values  are
based  on  a  statistical analysis of the treatability  data  for
benzo-(a)-pyrene obtained in the pilot study.   These two  values
account  for  variability  in  the pilot  study  and  variability
inherent in the operation of lime, settle, and filter technology.
                               656

-------
                PRIMARY ALUMINUM SUBCATEGORY    SECT  - V


 Potline scrubber liquor also contains treatable concentrations of
 toxic  metals  (most  notably  antimony  and   nickel),  fluoride,
 aluminum,  and suspended solids.  Treatment performance for these
 parameters was measured during the lime, settle, and filter tests
 performed for the PAH.   Results of the analyses are presented in
 Tables V-32 and V-33  (pages 716 - 717).

 As  shown  in  Table V-33,  BAT treatment  performance  for  the
 primary  aluminum subcategory was not achieved.   At   the  plant,
 potline   scrubber  liquor  is  processed  through  the   cathode
 reprocessing  circuit  to reduce  fluoride  concentrations.   The
 bleed  from  cathode  reprocessing  is then routed  back  to  the
 potline scrubbing circuit.   The cathode reprocessing wastewater,
 and  subsequently the potline scrubber liquor, contain  dissolved
 solids levels in the five to six percent range.  It appears  that
 this  significant matrix difference between cathode  reprocessing
 wastewater  and other plant raw wastewaters used to  develop  the
 treatment  performance  values  contributes  to  less   effective
 performance   of   the  treatment  technology.    Some   of   the
 ramification's of this finding are discussed in detail in  Section
 X of this supplement.

 Cyanide Treatment

 Prior   to  performing the pilot scale   work,   laboratory  (bench-
 scale)   studies  were performed to identify  the necessary reaction
 steps  and chemical  quantities  required to precipitate the  cyanide
 complexes  present in the  primary  aluminum wastewater matrix.    in
 general,  the  Agency found that  75  to 90  percent of  the  cyanide  is
 present  as   a   complex   hexacyanoferrate.     Thus,   the  primary
 function   of  the  laboratory work  was to  examine the   methods  and
 variables   affecting  the conversion  of  free    cyanide   and
 hexacyanoferrate  (III) complexes  to hexacyanoferrate (II)  so that
 cyanide  complexes   may   be precipitated as   prussian   blue.   A
 general description of the operating  procedures used in the  lab
 for  cyanide precipitation  is presented below:
      1.
      2.
      3.
      4.
      5.
      6.
      7.
      8.
Adjust pH to 9,
Add FeSO4,
Rapid mix,
Adjust pH (3 to 5),
Add FeSC-4, FeCl3,
Rapid mix for 10 minutes,
Settle for one hour, and
Filter (pressure).
Information obtained in the laboratory was then tested on a pilot
scale  level  at  a  primary aluminum  reduction  facility  using
cathode reprocessing wastewater.

Laboratory   work  performed  by  industry  on  cyanide   bearing
wastewaters  from  two  primary aluminum  plants  indicates  that
ferric chloride addition does not increase the amount of  cyanide
precipitated from the wastewater.   As the ferrous sulfate dosage
was  held constant,  the ferric chloride addition was varied with
                               657

-------
               PRIMARY ALUMINUM SUBCATEGORY   SECT - V
no  noticeable increase in cyanide removal.   This data tends  to
indicate that ferric chloride addition has little or no effect on
the precipitation of iron cyanide complexes.

The  Agency's pilot scale treatability studies revealed that  the
treatability   limits   for   cyanide   precipitation   are   not
transferable from coil coating to the primary aluminum wastewater
matrix.   The cryolite recovery operations discharge much  higher
concentrations  of  cyanide  than observed in  coil  coating  and
impair  treatment  by also discharging extremely  high  dissolved
solids  concentrations (five to six percent) that interfere  with
precipitation chemistry.

From  the  pilot  scale  work  it  was  determined  that  cyanide
precipitation can achieve 2.3 mg/1 cyanide,  and the addition  of
multimedia  filtration will further reduce cyanide to  1.1  mg/1.
Since  a  full  scale  cyanide precipitation  unit  is  not  used
anywhere  in the industry,  the mean variability factors obtained
from  the combined metals data base (CMDB) are used to  calculate
the  one-day  maximum and ten day  average  concentrations.   The
Agency received comments to the proposed regulation stating  that
the  transfer of the CMDB variability factors is not  appropriate
because  the precipitate formed during cyanide precipitation will
have  different settling characteristics than the lime and  metal
hydroxide sludge.   However,  since cyanide precipitation is  not
currently run at full scale, the CMDB variability factors will be
used due to the lack of any other data.
                               658

-------
          PRIMARY ALUMINUM SUBCATEGORY   SECT - V
                       TABLE V-l
WATER DISCHARGE RATES FOR ANODE AND CATHODE PASTE PLANT
               WET AIR POLLUTION CONTROL
                        (1/kkg)
  Plant Code

     353

     354

     365

     369
Percent     Production Normalized
Recycle        Discharge Flow

   0              2202

   0              1434

   0               754

   0               817
                          659

-------
                 PRIMARY  ALUMINUM SUBCATEGORY
                                       SECT  -  V
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                                                 660

-------
               PRIMARY ALUMINUM  SUBCATEGORY
                                                               SECT  -  V
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-------
               PRIMARY ALUMINUM SUBCATEGORY   SECT - v
                            TABLE V-3

           WATER DISCHARGE RATES FOR ANODE BAKE PLANT
                    WET AIR POLLUTION CONTROL
                    (1/kkg  of Anodes Baked)
Plant
Code   Furnace Type

354    Open top ring
       furnace

342    Tunnel kiln

343    Closed top
       ring furnace

364    Open top ring
       furnace

371    Open top ring
       furnace
 Scrubber Type

 Spray tower, wet
 ESP

Spray tower, dry

Venturi


Spray tower, dry


Wet ESP
        Production
        Normalized
Percent Discharge
Recycle    Flow
  99+


   0

   0


   0


  91
  728


11380

43235


  496


 1526
                              662

-------
PRIMARY ALUMINUM  SUBCATEGORY
                                       SECT  -  V
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-------
                PRIMARY ALUMINUM SUBCATEGORY
                                           SECT  -  V
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-------
               PRIMARY ALUMINUM SUBCATEGORY   SECT - V
                            TABLE V-5
                    WATER DISCHARGE RATE FOR
          ANODE CONTACT COOLING AND BRIQUETTE QUENCHING
       (1/kkg of Green Anodes or Briquettes Manufactured)
                                   Production Normalized
Plant Code Recycle
345*
349
353
354
35S
357
371
359*
360*
367
6101

96
0
NA
0
NA
100
0
0
0
97
NA
Discharge Flo\
988
9174
NA
1434
NA
0
1051
2711
1472
113
NA
* Briquette Quenching
                               665

-------
 PRIMARY ALUMINUM  SUBCATEGORY
                                                 SECT  -  V
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-------
               PRIMARY ALUMINUM  SUBCATEGORY
                                                               SECT  -  V
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-------
      PRIMARY ALUMINUM SUBCATEGORY   SECT - V
                   TABLE V-7

WATER DISCHARGE RATES FOR CATHODE REPROCESSING
        (1/kkg of Cryolite Production)
 Plant Code

      369

      363

      368

      370
Discharge Flow

     62050

      8400

     31700

     34540
                     668

-------
PRIMARY ALUMINUM SUBCATEGORY
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               PRIMARY ALUMINUM SUBCATEGORY   SECT - V
                            TABLE V-9

   WATER DISCHARGE RATES FOR POTLINE WET AIR POLLUTION CONTROL
             (1/kkg of Aluminum Reduction Production)
Plant     Cell
Code      Type      Scrubber Type

363       PB,       Solid cone spray,
          HSS       wet scrubber

369       HSS       Wet ESP

346       PS        Scrubbers, ESP

349       VSS       Venturi followed
                    by packed section

368       HSS       Wet ESP

370       HHS       Floating bed, wet
                    scrubbers

348       PB        Multiple cyclones
                    and floating bed

366       HSS       Wet ESP
         Production
         Normalized
Percent  Discharge
Recycle    Flow

  100          0
   91

    0

   96


   99 +

   99+


   NR


   NR
 592

2047

1160


1150

 463


  NR


  NR
NR — not reported
                               674

-------
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                                             SECT  -  V
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-------
                 PRIMARY ALUMINUM  SUBCATEGORY
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-------
              PRIMARY ALUMINUM SUBCATEGORY   SECT - V
                          TABLE V-ll
WATER DISCHARGE RATES FOR POTLINE SO2 WET AIR POLLUTION CONTROL
                  (1/kkg of Aluminum Reduced)
        Plant Code

         359

         360
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    77

    75
Discharge Flow

   1430

   1500
                              679

-------
               PRIMARY ALUMINUM SUBCATEGORY   SECT
          V
                           TABLE V-12

   WATER DISCHARGE RATES FOR POTROOM WET AIR POLLUTION CONTROL
            (1/kkg of Aluminum Reduction Production)
Plant     Cell
Code      Type      Scrubber Type

353       PB        104 low pressure
                    wet scrubber

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361       PB        NR

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         Production
         Normalized
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Recycle    Flow
   42


   98


   98


   99


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   93

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  1593


   568


  2790


    70


 25024

  1685

    NR

169000
                               680

-------
             PRIMARY ALUMINUM  SUBCATEGORY
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-------
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-------
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-------
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-------
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-------
               PRIMARY ALUMINUM SUBCATEGORY   SECT - V
                           TABLE V-14
  WATER DISCHARGE RATES FOR DEGASSING WET AIR POLLUTION CONTROL
             ((1/kkg of Aluminum Refined and Degassed)
Plant
Code
354
369
359
361*
Scrubber Type
Venturi
Packed Tower
ESP
NR
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         Normalized
Percent  Discharge
Recycle    Flow
0
0
0
NR
2840
1860
3130
NR
*Data reported with potline and potroom scrubbing and cannot  be
separated.
NR — Not reported
                               686

-------
              PRIMARY ALUMINUM  SUBCATEGORY
                                                 SECT - V
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-------
        PRIMARY ALUMINUM SUBCATEGORY   SECT - V
                    TABLE V-16

             WATER DISCHARGE RATES FOR
             POT REPAIR & POT SOAKING
     (1/kkg of Aluminum Reduction Production)
Plant Code

   349

   355

   356

   357

   358

   364

   365

   366

   369

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     100

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     100
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                        688

-------
        PRIMARY ALUMINUM SUBCATEGORY
                      SECT - V
                    TABLE V-17

             WATER DISCHARGE RATES FOR
             POT REPAIR & POT SOAKING
     (1/kkg of Aluminum Reduction Production)
Plant Code

   362
   355
   350

   340
   353
   345

   357
   352
   371

   369
   349
   351

   348
   365
   347

   360
   367
   359

   343
   370
   342

   361
   343
   366

   346
   6101
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      99+
      99
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      98
      94
      82

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       0

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       0

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       0
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      NA
      NA
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      NA
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   Discharge Flow

        123
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       2610

        600
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       6964

      12552
      15638
      23477

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      32860
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         NA
         NA
         NA

         NA
         NA
                         689

-------
        PRIMARY ALUMINUM SUBCATEGORY   SECT - V
                    TABLE V-18

             WATER DISCHARGE RATES FOR
       DIRECT CHILL CASTING CONTACT COOLING
            (ALUMINUM FORMING CATEGORY)
             (1/kkg of Aluminum Cast)
Plant Code

     1
     2
     3

     4
     5
     6

     7
     8
     9

    10
    11
    12

    13
    14
    15

    16
    17
    18

    19
    20
    21

    22
    23
    24

    25
    26
    27

    28
    29
    30

    31
    32
    33
Percent Recycle

      100
      100
       50

       97
      100
      100

      100
      100
      100

       99
       99
      100

       99
        0
       98

       97
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       98
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       94
       97
       99

       96
       96
       94

       92
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   Discharge Flow

          0
          0
          0

          0
          0
          0

          0
          0
          0

          0.2989
          0.3252
          0.4169

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        250.2
        313.4
        392.8

        496.2
        514.5
        612.9

        629.6
        779.7
        963.1

       1113
       1167
       1483

       1534
       1955
       2397

       2753
       3002
       4003
                        690

-------
        PRIMARY ALUMINUM SUBCATEGORY   SECT - V
              TABLE V-18 (Continued)

             WATER DISCHARGE RATES FOR
             POT REPAIR & POT SOAKING
     (1/kkg of Aluminum Reduction Production)
Plant Code

    34
    35
    36

    37
    38
    39

    40
    41
    42

    43
    45
    46

    47
    48
    49

    50
    51
    52

    53
    54
    55

    56
    56
    58

    59
    60
    61
Percent Recycle

        0
       NR
        0

        0
        0
        0

        0
        0
        0

        0
       98
       96

       NR
        0
        0

       NR
        0
       NR

        0
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       NR

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       NR

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       5041
       5337
       9089

       9506
      16590
      29390

      35500
      52540
      58370

      91310
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         NR

         NR
         NR
         NR

         NR
         NR
         NR

         NR
         NR
         NR

         NR
         NR
         NR

         NR
         NR
         NR
                        691

-------
               PRIMARY ALUMINUM SUBCATEGORY   SECT - V
                           TABLE V-19

                    WATER DISCHARGE RATES FOR
             CONTINUOUS ROD CASTING CONTACT COOLING
             (1/kkg of Aluminum Reduction Production)
       Plant Code

          346

          355

          362
                  Production Normalized
Percent Recycle      Discharge Flow
      NR

      99

      99 +
 NR

415

 11.3
nr — Not Reported
                               692

-------
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-------
               PRIMARY ALUMINUM  SUBCATEGORY
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-------
PRIMARY ALUMINUM SUBCATEGORY
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-------
                PRIMARY ALUMINUM SUBCATEGORY   SECT - V
                            TABLE V-28

         REPORTED PRESENCE OR ABSENCE OF TOXIC POLLUTANTS
                       (From Dcp Responses)
 Pollutant
 Acenaphthene
 Pluoranthene
 1,2-benzanthracene
 Benzo(a)pyrene
 Chrysene
 Pyrene
 3,4-benzofluoranthene
 Benzo(k)fluoranthene
 Acenaphthylene
 Anthracene
 Benzo(ghi)pe rylene
 Fluorene
 Phenanthrene
 Dibenzo(a,h)anthracene
 Indeno(1,2,3-cd)pyrene
 Methyl  bromide
 Naphthalene
 Pentachlorophenol
 Tetrachloroethylene
 Toluene
 Antimony
 Arsenic
 Cadmium
 Chromium
 Copper
 Cyanide
 Lead
Mercury
Nickel
 Selenium
Silver
Thallium
Zinc
Known
Present
0
0
0
0
1
0
0
0
0
0
0
2
0
0
0
0
0
0
0
0
0
3
5
6
7
16
1
1
1
1
1
0
8
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4
6
8
8
7
8
5
5
5
9
5
8
9
4
4
1
6
1
0
1
2
3
2
3
5
4
5
3
3
1
3
0
3
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20
19
19
19
20
19
22
22
21
19
22
18
19
23
23
26
21
27
27
27
21
17
16
16
14
5
19
21
23
22
22
24
16
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2
0
0
0
0
0
0
1
0
0
0
0
0
0
1
1
0
1
0
4
4
4
2
1
0
2
2
0
3
1
2
—
                               712

-------
     PRIMARY ALUMINUM SUBCATEGORY
              SECT - V
                 Table V-29
        SOURCE WATER CHARACTERISTICS
 Parameter

Sb
CN (T)
Ni

TSS
O & G
pH (std units)

Aluminum
Calcium
Chloride

Fluoride
Iron
Total Dissolved Solids
Alkalinity (as CaC03)
Concent ration (mg/1)

        0.015
       <0.01
        2.
        1
        6.95
       50
       36

        0.34
        0.80
      273
      198
                     713

-------
             •PRIMARY  ALUMINUM SUBCATEGORY    SECT - V
                          Table V-30

 RAW WASTEWATER  CHARACTERISTICS  — POTLINE SCRUBBER SLOWDOWN
                      No.
     Parameter      Values

Sb                   10
CN  (T)               10
Ni                   10

TSS                  10
O & G                 5
pH  (std units)

Aluminum            ip
Calcium              9
Chloride             9

Fluoride            10
Iron                 9
Total Dissolved     10
  Solids (Percent)

Alkalinity          9
  (as CaCOs)
Turbidity (NTU)    10
Temperature (°C)   10
     Concentration (mg/1)
   Average            Range
    4.68
   38.9
    1.0

  130
    9
   24
    3.7
 1275

  874
   12.1
    6.18
5300

   3.8
  34.5
1.1.3 - 10.0
27.4 - 47.5
0.70 - 1.40
  75
   6
 8.0

  20
 1.5
1200

 237
 9.5
5.02
238
14
9.42

27
9
1400

1260
16
6.74
4900 - 7300
 3.2
33.3
4.6
37.2
                             714

-------
               PRIMARY ALUMINUM SUBCATEGORY
            SECT - V
                           Table V-31

           CONCENTRATION OF PAH IN POTLINE WASTEWATER
          PAH
   Napthalene
   Acenapthylene
   Acenapthene

   Fluorene
   Phenanthrene &
      Anthracene
   Fluoranthene

   Pyrene
   Chrysene &
      Benzo(a)anthracene
   3,4-Benzofluoranthene &
      Benzo(k)fluoranthene

   Benzo(a)pyrene
   Dibenzo(a,h)anthracene

   Indeno(l,2f3-cd)pyrene
   Benzo(ghi)perylene
                                    Concentration (mg/1)
Average
  ND
  ND
0.030

  ND
  ND

2.740

2.000
2.230

0.790
1.100
0.140

  ND
0.310
     Range
      ND
      ND
 0.02 - 0.040

      ND
      ND

1.840 - 3.670

1.410 - 2.900
1.780 - 3.200

0.600 - 1.060
0.700 - 1.820
0.090 - 0.200

      ND
0.220 - 0.440
NOTES:
  ND - Not Detected (quantification limit = 0.010 mg/1)
  All values reported in mg/1 without correction for recovery
  Analysis by Method 625.
  Average derived from 9 data points.
                               715

-------
               PRIMARY ALUMINUM SUBCATEGORY   SECT - V
                           Table V-32
               SAMPLE DATA SUMMARY OF PAH ANALYSIS
                     Potline Scrubber Liquor

                               Clarifier    Filter
      PAH                      Effluent    Effluent
   Naphthalene                   ND          ND
   Acenaphthylene                ND          ND
   Acenaphthene                0.010       0.010

   Fluorene                      ND          ND
   Phenanthrene &                ND          ND
      Anthracene
   Fluoranthene                0.170       0.114

   Pyrene                      0.110       0.079
   Chrysene &                  0.040       0.023
      Benzo(a)anthracene
   3,4-Benzofluoranthene &     0.020       0.010
      Benzo(k)fluoranthene

   Benzo(a)pyrene              0.020       0.010
   Dibenzo(a,h)anthracene        ND          ND

   Indeno(l,2,3-cd)pyrene        ND          ND
   Benzo(ghi)perylene            ND          ND
Act. Carbon
 Effluent
   ND
   ND
   ND

   ND
   ND

   ND

   ND
   ND

   ND
   ND
   ND

   ND
   ND
NOTES:
  ND - Not Detected (quantification limit = 0.010 mg/1)
  All values reported in mg/1 without correction for recovery
  Analysis by Method 625.
  Average derived from 8 clarifier data points and 9 filter
     effluent data points.
                               716

-------
           PRIMARY ALUMINUM SUBCATEGORY
                      SECT - V
                       Table V-33
           SAMPLE DATA SUMMARY OF METALS ANALYSIS
                 Potline Scrubber Liquor
Parameter

 Antimony

 Nickel

 Aluminum

 Fluoride

 TSS
Clarifier
Effluent

  3.3

  0.58

  2.2

212

 82
 Filter
Effluent

  2.99

  0.57

  1.9

206

 15
                           717

-------
           PRIMARY ALUMINUM SUBCATEGORY    SECT - V

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Code Number
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             SAMPLING SITES AT PRIMARY ALUMINUM  PLANT A
aThis plant uses  the VSS cell configuration, however,  the paste

 is formed into briquettes for insertion  into  the  carbon anode.
                               718

-------
PRIMARY ALUMINUM SUBCATEGORY
SECT - V
Spent
Pot
Linings

Pot line
Air
Pollution
Control


n

. n^a w

Cryolite
Recovery
Thickener
Underflow
CT> 1V\ /
                  Excess
                  Well Water
                  0.29 MGD
                          0.37 MGD
     Lime Tray
   .J Thickener
    I Underflow
     0.022 MGD
Acid
(H2S04)
Neutrali-
zation


Pond
                                                 0.37 MGD
Non-
Contact
Cooling
Water

Contact
Cooling
Water
Slowdown
<•*•>-"! 't
A26\
f?\ »
(&) *
0.22 MGD
Y
Discharge
fc
                     Figure  V-2

  SAMPLING SITES AT PRIMARY ALUMINUM  PLANT  B
                        719

-------
PRIMARY ALUMINUM SUBCATEGORY
SECT - V
                    VOA Blank
                                            Discharge
                   Figure V-3



  SAMPLING SITES  AT PRIMARY ALUMINUM PLANT C
                     720

-------
         PRIMARY ALUMINUM SUBCATEGORY
                      SECT -  V
  Potroom Air
   Pollution
Control Cryolite
     Kiln
                            Sludge
                            Recycle
                   1.3 MGD
Mix Tank
   &
Settling
Recycle
     Storm
     Water
    Anode
   Contact
   Cooling
   Anode Paste
 Plant Scrubber
    Liquor
                                 Decant
                                  Pond
            0.15
            MGD
   Anode Bake
   Plant Air
Pollution Control
                To Potroom
                 Scrubber
 Decant
  Pond
  Noncontact
   Cooling
   Slowdown
             Oil
             for
      Reclamation
 Casting Contact
  Cooling Water
                            Surge
                            Pond
                                                                        1.6 MGD
                   Emergency Overflow
                                  Figure  V-4

           SAMPLING  SITES  AT PRIMARY ALUMINUM  PLANT  D
                                     721

-------
       PRIMARY ALUMINUM SUBCATEGORY
SECT - V
   146\
VGA Blank
Rectifier
Cooling
Water

Steam
Boiler
Slowdown

Anode
Paste
Plant

Cathode
Storage

Pot line Air
Pollution
Control

Refining and
Degassing
Air Pollu-
tion Control

Casting
Contact
Cooling
Water




AA fc
vV/
0.0864 MGD
A?N ^
\
-------
PRIMARY  ALUMINUM  SUBCATEGORY
SECT - V
                                      VGA Blank
               Recycle With Caustic Soda Addition
1
t
Anode Bake
Plant Air
Pollution
Control
1.03 MGD

Settling
With
Polymer
Addition

                     0.202 MGD
                                  T
                                 Sludge
                                   to
                                Off-Site
                                Disposal
                               Discharge
                                                   Discharge
                                           0.094 MGD
                     Figure  V-6

  SAMPLING SITES AT  PRIMARY ALUMINUM PLANT F
                        723

-------
PRIMARY ALUMINUM  SUBCATEGORY    SECT  -  V
THIS PAGE INTENTIONALLY LEFT BLANK
               724

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              PRIMARY ALUMINUM SUBCATEGORY
SECT - VI
                           SECTION VI

                SELECTION OF POLLUTANT PARAMETERS
This section examines chemical analysis data presented in Section
V  from primary aluminum  plants and discusses the  selection  or
exclusion of pollutants for potential limitation.  The basis  for
the  regulation  of toxic and other pollutants  is  discussed  in
Section  VI of the General Development Document (Vol I) and. each
pollutant  selected for potential limitation is discussed  there.
That   discussion  provides  information  concerning  where   the
pollutant  originates (i.e., whether it is a naturally  occurring
substance, processed metal, or a manufactured compound);  general,
physical properties and the form of the pollutant; toxic  effects
of the pollutant in humans and other animals; and behavior of the
pollutant  in POTW at the concentrations expected  in  industrial
discharges. •

The  discussion  that  follows describes the  analysis  that  was
performed   to   select   or  exclude  pollutants   for   further
consideration  for  limitations and  standards.   Pollutants  are
selected  for  further  consideration  if  they  are  present  in
concentrations  treatable by the technologies considered in  this
analysis.  The treatable concentrations used for the toxic metals
were   the  long-term  performance  values  achievable  by   lime
precipitation,  sedimentation,  and  filtration.   The  treatable
concentrations   for  the  toxic  orgartics  were  the   long-term
performance values achievable by carbon adsorption.

After proposal, the Agency re-evaluatecl the treatment performance
of   activated  carbon  adsorption  to  control   toxic   organic
pollutants.  The treatment performance for the acid  extractable,
base-neutral  extractable,  and volatile organic  pollutants  has
been  set equal to the analytical quantification limit  of  0.010
mg/1.   The  analytical quantification limit for  pesticides  and
total phenols (by 4-AAP method) is 0.005 mg/1, which is below the
0.010 mg/1 accepted for the other toxic organics.  However, to be
consistent,  the treatment performance of 0.010 mg/1 is used  for
pesticides  and total phenols.  The 0.010 mg/1  concentration  is
achievable,  assuming enough carbon is used in the column  and   a
suitable  contact time is allowed.  The frequency  of  occurrence
for 36 of the toxic .pollutants has been redetermined based on the
revised  treatment performance value.  As a result,  naphthalene,
which was not selected at proposal, has been selected  for further
consideration for limitation.

CONVENTIONAL AND NONCONVENTIONAL POLLUTANT PARAMETERS

This   study   considered  samples  from  the  primary   aluminum
subcategory for three conventional pollutant parameters  (oil  and
grease,  total suspended solids,  and pH) and  six nonconventional
pollutant parameters  (aluminum,  ammonia, chemical oxygen demand,
                                725

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               PRIMARY ALUMINUM SUBCATEGORY   SECT - VI


 chloride,  fluoride, total organic carbon,  and total phenols).

 CONVENTIONAL AND NONCONVENTIONAL POLLUTANT PARAMETERS SELECTED

 The  conventional  and nonconventional pollutants  and  pollutant
 parameters  selected  for  consideration for limitation  in  this
 subcategory are:

      aluminum
      fluoride
      total suspended solids (TSS)
      oil and grease
      pH

 Aluminum   is  selected for consideration for limitation  for   two
 reasons:    (1)   it   is  the  major  product  of   plants  in  this
 subcategory,  and  (2) it was found at concentrations higher  than
 those  achievable by identified treatment  technology (1.49  mg/1)
 in three of four samples from three plants.

 Fluoride is found primarily in wastewaters from  wet scrubbing   of
 gases  from  the primary  reduction  of  alumina  to   aluminum.
 Fluorides   were   measured above the concentration  attainable   by
 identified  treatment technology (14.5 mg/1)  in  12  of 16 samples
 from   seven plants.    Treatable concentrations ranged from  63   to
 13,000 mg/1.   Therefore,   fluoride is selected  for consideration
 for limitation.
Total suspended  solids  ranged  from  4  to  54,500 mg/1.
18 samples had concentrations  above that achievable
treatment  technology   (2.6  mg/1).   Furthermore,
technologies  used to remove toxic  metals do so by
the metals.   A  limitation on  total suspended solids
sedimentation to remove precipitated  toxic metals is
operating.   Therefore,  total  suspended solids is
consideration for limitation.
  Eighteen of
by identified
most  of  the
precipitating
 ensures that
  effectively
selected  for
Oil  and grease concentrations in the wastewaters sampled  ranged
from  2 to 1,400 mg/1 in 18 samples.   The processing of coal tar
pitch  and  coke in the anode paste and bake  operations  is  the
principal source of these pollutants.  The concentration in 12 of
the  18  samples exceeded the treatable concentration (10  mg/1).
Thus,   this   pollutant   is  selected  for  consideration   for
limitation.

The  pH  values  observed ranged from  5.0  to  11.0.   Effective
removal of toxic metals by precipitation requires careful control
of  pH.   Therefore,  pH  is considered for  limitation  in  this
subcategory.

TOXIC POLLUTANTS

The  frequency  of  occurrence  of the toxic  pollutants  in  the
wastewater  samples taken is presented in Table VI-1 (page  735).
These  data provide the basis for the categorization of  specific
                               726

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              PRIMARY ALUMINUM SUBCATEGORY   SECT - VI
pollutants,  as discussed below.  Table VI-1 is based on the  raw
wastewater  data from streams 145, 194, 26, 195, 126,  127,  142,
144,  28,  150, 137, and 135 (see Section  V).   Treatment  plant
samples  and  samples  containing nonscope  wastewater  were  not
considered in the frequency count.

TOXIC POLLUTANTS NEVER DETECTED

The  toxic pollutants listed   in Table VI-2 (page 739) were  not
detected  in  any  wastewater  samples  from  this   subcategory;
therefore,   they   are  not  selected   for   consideration   in
establishing regulations:


TOXIC POLLUTANTS NEVER FOUND ABOVE THEIR ANALYTICAL
QUANTIFICATION LEVEL

Toxic   pollutants   which  are  not  detectable  include   those
pollutants   whose  concentrations  fall  below   EPA's   nominal
detection  limit.   The toxic pollutants  listed  in  Table  VI-3
(page 741) were never found above their analytical quantification
concentration  in any wastewater samples from  this  subcategory;
therefore,   they   are  not  selected   for   consideration   in
establishing regulations.

TOXIC POLLUTANTS PRESENT BELOW CONCENTRATIONS ACHIEVABLE BY
TREATMENT

The  pollutant  mercury  is  not selected  for  consideration  in
establishing  limitations  because  it  was  not  found  in   any
wastewater  samples  from this subcategory  above  concentrations
considered   achievable   by  existing  or  available   treatment
technologies.  Mercury was detected at, or above, its 0.0001 mg/1
analytical  quantification limit in three of 18 samples  from  10
plants.  All of the values are below the 0.026 mg/1 concentration
considered   achievable   by  identified  treatment   technology.

TOXIC POLLUTANTS DETECTED IN A SMALL NUMBER OF SOURCES

Toxic  pollutants  detectable in the effluent from only  a  small
number  of sources within the subcategory and uniquely related to
only  those  sources  are not appropriate  for  limitation  in  a
national  regulation.  The pollutants listed in Table VI-4  (page
735)  were not selected for further consideration for  limitation
on this basis.

Although these pollutants were not selected for consideration  in
establishing nationwide limitations,  it may be appropriate, on a
case-by-case  basis,  for  the local  permit  writer  to  specify
effluent limitations.

Benzene was detected in four of eight samples collected from  six
plants.  Two of the detected concentrations were below analytical
quantification  level.   The other two concentrations were  0.013
mg/1  and  0.016 mg/1,  which are slightly  above  the  treatable
                               727

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               PRIMARY ALUMINUM SUBCATEGORY   SECT  -  VI
 concentration.     These  two  samples   detected   above   treatable
 concentrations   were found at  the same  plant  in  two  different  raw
 wastewaters.    The same streams  in another  plant did not  contain
 benzene.    For   these  reasons,  benzene  is  not  considered   for
 limitation.

 2-Chloronaphthalene    was  measured    above   its     analytical
 quantification   limit  in just one of 19 samples collected at   10
 plants.    The reported  value was 0.041  mg/1;   this pollutant   was
 not   detected   in  any of the other 18 samples.    Because  it   was
 found at  just  one plant,   2-chloronaphthalene is not   considered
 for  limitation.

 Chloroform, a common laboratory  solvent,  was  detected in three of
 eight samples collected from six plants.    Only  one  concentration
 was   above the  analytical  quantification limit and this was above
 the  treatable concentration.   This pollutant is not attributable
 to   specific materials  or  processes associated with  the  primary
 aluminum   subcategory.    Sample   contamination   is  the  probable
 source of  this  pollutant;  therefore, chloroform  is not  considered
 for  limitation.

 Bis(2-chloroisopropyl)   ether  was found  above  its   analytical
 quantification   limit  in  just one of 19  samples collected at   10
 plants.    This   pollutant  was  not detected  in 17  other  samples.
 Therefore,  bis(2-chloroisopropyl)  ether   is not  considered   for
 limitation.

 Methylene  chloride was  detected  in two  of eight  samples from   six
 plants.    Only    one  concentration  was   above  the   analytical
 quantification   limit   and   this was   above    the    treatable
 concentration.   The   reported  value (0.055  mg/1)  was from potrpom
 wet   air pollution control  raw  wastewater.   Methylene  chloride
 from  this  stream  at   another  plant   was  not   detected.   This
 pollutant  is not attributable  to specific materials  or   processes
 associated with  the  primary aluminum subcategory,  but is  a common
 solvent  used   in   analytical  laboratories.   There  is   a  high
 probability   of.  sample   contamination.    For   these    reasons,
 methylene chloride  is not  considered for  limitation.

 N-nitrosodiphenylamine   was   detected  above    its    analytical
 quantification   limit   in  only   one of  19  samples   taken  at  10
 plants.   The  detected  concentration was 0.057  mg/1.   Although
 this   value  is  above  the 0.010  mg/1   considered  attainable  by
 identified  treatment technology,  N-nitrosodiphenylamine  is   not
 considered for limitation because  it was found above a   treatable
 concentration at only one plant.

Phenol  was detected above its analytical quantification  limit in
only  one  of six  samples taken  from two  plants.   Although   the
 0.070  mg/1  concentration  observed  is  above  the  0.010  mg/1
 treatable concentration,  phenol  is not considered for  limitation
because it was found at only one plant.

Bis(2-ethylhexyl)   phthalate  was  found  above   its   analytical
                               728

-------
              PRIMARY ALUMINUM SUBCATEGORY
SECT - VI
quantification  limit in 12 of 19 samples from  10  plants.   The
concentrations  observed  ranged from 0.011 to  2.50  mg/1.   The
presence  of this pollutant is not attributable to  materials  or
processes  associated with the primary aluminum subcategory.   It
is  commonly  used  as  a plasticizer  in  laboratory  and  field
sampling  equipment.  EPA  suspects sample contamination  as  the
source of this pollutant.  Therefore, bis(2-ethylhexyl) phthalate
is not considered for limitation.

Butyl   benzyl   phthalate  was  found   above   its   analytical
quantification  limit in four of 19 samples from 10 plants.   The
concentrations ranged from 0.012 to 0.085 mg/1.   The presence of
this  pollutant  is not attributable to  materials  or  processes
associated with the primary aluminum subcategory.  It is commonly
used as a plasticizer in laboratory and field sampling equipment.
EPA   suspects  sample  contamination  as  the  source  of   this
pollutant.  Therefore,  butyl  benzyl phthalate is not considered
for limitation.

Di-n-butyl    phthalate   was   found   above   its    analytical
quantification limit in three of 19 samples from 10 plants.   The
concentrations observed ranged from 0.022 to 0.126 mg/1.   Two of
the  three  samples showed concentrations above  the  0.010  mg/1
treatable  concentration.   The presence of this pollutant is not
attributable  to  materials  or  processes  associated  with  the
primary  aluminum  subcategory.    It  is  commonly  used  as   a
plasticizer  in  laboratory and field  sampling  equipment.   EPA
suspects  sample  contamination as the source of this  pollutant.
Therefore, di-n-butyl phthalate is not considered for limitation.

3,4-Benzofluoranthene   was   detected   above   its   analytical
quantification  limit in just one of 19 samples from  10  plants.
Since  it was found in only one plant,  3,4-benzofluoranthene  is
not considered for limitation.

Benzo(k)fluoranthene  was also found above its analytical  quanti
fication limit in just one of 19 samples.   Therefore,  benzo(k)-
fluoranthene is not considered for limitation.

Acenaphthylene  was  detected in six of 19 samples from 10  waste
streams   sampled.    This   pollutant  was  present  below   the
quantification  limit in five of the samples.   Only  one  sample
contained a treatable concentration of acenaphthylene.   Since it
was  found  treatable at only one plant,  acenaphthylene  is  not
considered for limitation.

Indeno(1,2,3-cd)pyrene   was   detected  above   its   analytical
quantification  limit in two of 19 samples taken from 10  plants.
Since it was found in only two plants,  indeno(l,2,3-cd)pyrene is
not considered for limitation.

The first group of PCB's (polychlorinated biphenyls) was detected
above its analytical quantification limit in one of three samples
taken  at three plants.    The group contains PCB-1242,  PCB-1254,
and  PCB-1221,  which  are reported together since they  are  not
                               729

-------
              •PRIMARY ALUMINUM SUBCATEGORY   SECT - VI
clearly separated by the analytical protocol used in this  study.
Because  these  pollutants  were detected in a  small  number  of
sources, they are not considered for limitation.

Beryllium  was found above its analytical quantification limit in
12  of 21 samples taken from 10  plants.   Concentrations  ranged
from 0.02 to 0.4 mg/1.  Only one sample contained a concentration
above   the   0.20  mg/1  considered  attainable  by   identified
technology.  Because it was found at a treatable concentration at
only one plant, beryllium is not considered for limitation.

Silver was measured above its analytical quantification limit  in
10   of   21  samples.    Three   samples   contained   treatable
concentrations  of  silver,  all  measured  at  the  same  plant.
Therefore, silver is not considered for limitation.

TOXIC POLLUTANTS SELECTED FOR FURTHER CONSIDERATION FOR
LIMITATION

The  toxic  pollutants  listed  below are  selected  for  further
consideration  in establishing limitations for this  subcategory.
The  toxic pollutants selected are each discussed  following  the
list.

       1.  acenaphthene
      39.  fluoranthene
      55.  naphthalene
      72.  benzo(a)anthracene
      73.  benzo(a)pyrene
      76.  chrysene
      78.  anthracene     (a)
      79.  benzo(ghiJperylene
      80.  fluorene
      81.  phenanthrene   (a)
      82.  dibenzo(a,h)anthracene
      84.  pyrene
     114.  antimony
     115.  arsenic
     116.  asbestos
     118.  cadmium
     119.  chromium
     120.  copper
     121.  cyanide
     122.  lead
     124.  nickel
     125.  selenium
     128.  zinc

(a)  Reported together as a combined value.

Acenaphthene  was found above its analytical quantification limit
in 14 of 19 samples from 10 plants,  with concentrations  ranging
from 0.011 to 29.0 mg/1.  Ten of those samples, representing five
plants,  were  above  the 0.010 mg/1 concentration attainable  by
identified  treatment  technology.   Therefore,  acenaphthene  is
                               730

-------
              PRIMARY ALUMINUM SUBCATEGORY   SECT - VI
selected for further consideration for  limitation.

Fluoranthene  was  measured above its  analytical  quantification
limit  in  15  of 19 samples from 10 plants  with  concentrations
ranging from 0.073 to 32.0 mg/1.   All 15  samples,  representing
seven  plants,  were  above  the 0.010  treatable  concentration.
Therefore, fluoranthene is selected for further consideration for
limitation.

Naphthalene  was detected in 11 of 19 samples collected  from  10
plants.   Seven  of the 11 detected concentrations were above the
treatable  concentration  (0.010 mg/1) attainable  by  identified
treatment technology.  These concentrations ranged from 0.02 mg/1
to 7.7 mg/1.  Seven of the 10 raw wastewater streams sampled were
found to contain naphthalene.  Therefore, naphthalene is selected
for further consideration for limitation.

Benzo(a)anthracene was found above its analytical  quantification
limit  in  15  of  19  samples,   taken  from  10  plants,   with
concentrations  ranging  from  0.014  to  14.0  mg/1.    Fourteen
samples,  representing  seven plants,  were above the 0.010  mg/1
range  considered attainable by identified treatment  technology.
Therefore,    benzo-(a)anthracene   is   selected   for   further
consideration for limita-tion.

Benzo(a)pyrene  was  found  above its  analytical  quantification
limit  in  13  of  19  samples,   taken  from  10  plants,   with
concentrations ranging from 0.017 to 11.0 mg/1.   Twelve samples,
representing   six  plants,   were  also  above  the  0.010  mg/1
concentration  considered  attainable  by  identified   treatment
technology.   Therefore,  benzo(a)pyrene  is selected for further
consideration for limitation.

Chrysene  was measured above its analytical quantification  limit
in 15 of 19 samples,  taken from 10 plants,  with  concentrations
ranging  from  0.030  to  30.0  mg/1.   There  were  14  samples,
representing  seven plants,  above the 0.010  mg/1  concentration
considered   attainable  by  identified   treatment   technology.
Therefore,  chrysene  is  selected for further consideration  for
limitation.

The toxic pollutants anthracene and phenanthrene are not  clearly
separated  by the analytical protocol used in this  study;  thus,
they  are  reported together.   The sum of these  pollutants  was
measured   at  concentrations  greater  than   their   analytical
quantification limit in 12 of 19 samples, collected at 10 plants,
with  concentrations ranging from 0.029 to 22.0 mg/1.   Eleven of
the 12 samples,  representing five plants,  were above the  0.010
mg/1   treatable  concentration.    Therefore,   anthracene   and
phenanthrene   are   selected  for  further   consideration   for
limitation.

Benzo(ghi)perylene was found above its analytical  quantification
limit  in  six  of  19  samples,   taken  from  10  plants,  with
concentrations ranging from 0.019 to  2.40 mg/1.    Five of the six
                               731

-------
              PRIMARY ALUMINUM  SUBCATEGORY
SECT - VI
 samples,   representing   four  plants,  were above  the  0.010  mg/1
 concentration  attainable  by   identified  treatment   technology.
 Therefore,    benzo-(ghi)perylene    is   selected   for    further
 consideration for  limitation.

 Fluorene   was measured above its analytical quantification limit
 in nine of  19 samples,   taken from 10 plants, with concentrations
 ranging from 0.039 to 5.30 mg/1.   All nine samples, representing
 four plants,  were above the 0.010 mg/1 concentration  attainable
 by  identified  treatment  technology.   Therefore,  fluorene   is
 selected for further consideration for limitation.

 Dibenzo(a,h)anthracene    was   found   above   its    analytical
 quantification limit in  five of 19 samples, taken  from 10  plants,
 with  con  centrations ranging from 0.012 to 1.9 mg/1.   All  five
 samples,   representing   four plants,  were above the   0.010  mg/1
 concentration  attainable  by   identified  treatment   technology.
 Therefore,   dibenzo(a,h)anthracene   is  selected for    further
 consideration   for  limitation.

 Pyrene was  found above its analytical quantification limit in   16
 of 19 samples,  taken from 10 plants, with concentrations  ranging
 from  0.05  to 34.0 mg/1.   All 16   samples,  representing  eight
 plants,  were  above  the 0.010 mg/1 concentration attainable   by
 identified  treatment technology.   Therefore,  pyrene  is selected
 for further consideration for limitation.

 Antimony  was measured above its analytical quantification  limit
 in 14 of 21 samples,  taken from 11 plants,  with  concentrations
 ranging from 0.05 to 1.5 mg/1.   Since five samples, representing
 three  plants,  were  also  above  the  0.47  mg/1  concentration
 attainable  by  identified  treatment  technology,   antimony   is
 selected for further consideration for limitation.   Selection  of
 antimony  is  further  justified based  on  the  analytical  data
 collected  during  the Agency's pilot scale  treatability  study.
 Antimony was found in 10 of 10 samples all above 1 mg/1.

 Arsenic was found above  its analytical quantification  limit in  17
 of 21 samples,  taken from 11 plants, with concentrations  ranging
 from 0.006 to 1.5 mg/1.  Seven samples, representing five plants,
 were  above the 0.043 mg/1 concentration attainable by identified
 treatment technology.  Therefore, arsenic is selected  for  further
 consideration for limitation.

Asbestos    (chrysotile)   was  measured  above   its   analytical
 quantification  limit  in the one raw wastewater sample  analyzed
 for  this pollutant.   The measured value was 310 million  fibers
per  liter  (MFL)   which is well above the value  of   10  million
 fibers attainable by the identified treatment technology.  At the
plant  where  it  was detected,   both the source  water  and  the
wastewater  discharge  contained  negligible  concentrations   of
asbestos.   Asbestos is considered for further limitation since  it
was  detected above a treatable concentration in the only  sample
 it was analyzed for.
                               732

-------
              PRIMARY ALUMINUM SUBCATEGORY   SECT - VI
Cadmium was measured above its analytical quantification limit in
10  of  21 samples,  taken from 11  plants,   with  concentrations
ranging  from 0.0026 to 0.2 mg/1.    Eight  samples,  representing
four plants,  were above the 0.049 mg/1 concentration  attainable
by  identified  treatment  technology.     Therefore,   cadmium  is
selected for further consideration for  limitation.

Chromium  was found above its analytical quantification limit  in
17  of  21 samples,  taken from 11  plants,   with  concentrations
ranging from 0.006 to 6.0 mg/1.   Three samples,  representing two
plants,  were  above  the 0.07 mg/1 concentration  attainable  by
identified treatment technology.  Therefore, chromium is selected
for further consideration for limitation.

Copper was measured above its analytical quantification limit  in
20  of  21  samples, taken from 11  plants,   with  concentrations'
selected for further consideration for  limitation.

Lead   was .  found  in  concentrations    above   its    analytical
quantification  limit in 15 of 21 samples,  taken from 11 plants,
with  concentrations  ranging from 0.008  to  5.0  mg/1.   Twelve
samples,     representing  six plants,  were above the  0.08  mg/1
concentration  attainable  by  identified  treatment   technology.
Therefore,  lead  is  selected  for  further  consideration   for
limitation.

Cyanide was found above its analytical  quantification limit in 20
of 22 samples, taken from 12 plants, with concentrations  ranging
from  0.002  to 180.0 mg/1. Since 10 samples,  representing  five
plants, were also above thel.l mg/1 concentrations attainable  by
identified  treatment  technology (refer to Section VII  -  Pilot
Scale  Treatability  Study),  cyanide  is  selected  for  further
consideration for limitation.

Nickel was measured above its analytical quantification limit  in
17  of  21 samples,  taken from 11  plants,   with  concentrations
ranging from 0.014 to 4.0 mg/1.   Since 11- samples,  representing
six   plants,   were  also  above  the   0.22  mg/1  concentration
attainable by identified treatment technology, nickel is selected
for further consideration for limitation.  Selection of nickel is
further  justified based on the analytical data collected  during
the Agency's pilot scale treatability study.  Nickel  was found in
10 of 10 samples all greater than 0.22  mg/1.

Selenium  was found above its analytical quantification limit  in
14  of  21 samples,  taken from 11  plants,   with  concentrations
ranging from 0.01 to 44.0 mg/1.   Eight samples,  representing two
plants,  were above the 0.20 mg/1 concentration attainable by the
identified treatment technology.  Therefore, selenium is selected
for further consideration for limitation.

Zinc   was   measured   above   its   analytical   quantification
concentration  in  18 of 21 samples taken from  11  plants,  with
concentrations  ranging from 0.01 to 1.0  mg/1.   Seven  samples,
representing three plants, were above the 0.23 mg/1 concentration
                               733

-------
              PRIMARY ALUMINUM SUBCATEGORY   SECT - VI
attainable  by the identified treatment  technology.   Therefore,
zinc is selected for further consideration for limitation.
                              734

-------
               PRIMARY  ALUMINUM SUBCATEGORY
                                                            SECT -  VI
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-------
               PRIMARY  ALUMINUM SUBCATEGORY
                                                   SECT - VI
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                                      736

-------
              PRIMARY  ALUMINUM  SUBCATEGORY
                                                     SECT -  VI
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-------
PRIMARY ALUMINUM SUBCATEGORY
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                    738

-------
        PRIMARY ALUMINUM SUBCATEGORY   SECT - VI
                     TABLE VI-2

           TOXIC POLLUTANTS NEVER DETECTED

 2.   acrolein
 3.   acrylonitrile
 5.   benzidene
 6.   carbon tetrachloride
 7.   chlorobenzene
 8.   I/2,4-trichlorobenzene
 9.   hexachlorobenzene
10.   1,2-dichloroethane
11.   1,1,1-trichloroethane
12.   hexachloroethane
13.   1,1-dichloroethane
14.   1,1,2-trichloroethane
15.   1,1,2,2-tetrachloroethane
16.   chloroethane
17.   DELETED
18.   bis(2-chloroethyl) ether
19.   2-chloroethyl vinyl ether
21.   2,4,6-trichlorophenol
22.   parachlorometa cresol
24.   2-chlorophenol
25.   1,2-dichlorobenzene
26.   1,3-dichlorobenzene
27.   1,4-dichlorobenzene
28.   3,3'-dichlorobenzidiene
29.   1,1-dichloroethylene
30.   1,2-trans -dichloroethylene
31.   2,4-dichlorophenol
32.   1,2-dichloropropane
33.   1,3-dichloropropylene
34.   2,4-dimethylphenol
35.   2,4-dinitrotoluene
36.   2,6-dinitrotoluene
37.   I/2-diphenylhydrazine
38.   ethylbenzene
40.   4-chlorophenyl phenyl ether
41.   4-bromophenyl phenyl ether
43.   bis(2-chloroethoxy) methane
45.   methyl  chloride
46.   methyl  bromide
47.   bromoform
48.   dichlorobromomethane
49.   DELETED
                          739

-------
         PRIMARY ALUMINUM SUBCATEGORY   SECT - VI
                TABLE VI-2 (Continued)

            TOXIC POLLUTANTS NEVER DETECTED

 50.  DELETED
 51.  chlorodibromomethane
 52.  hexachlorobutadiene
 53.  hexachlorocyclopentadiene
 56.  nitrobenzene
 57.  2-nitrophenol
 58.  4-nitrophenol
 59.  2,4-dinitrophenol
 60.  4,6-dinitro-o-cresol
 61.  N-nitrosodimethylamine
 63.  N-nitrosodi-n-propylamine
 64.  pentachlorophenol
 71.  dimethyl phthalate
 85.  tetrachloroethylene
 88.  vinyl chloride
129.  2,3,7,8-tetrachlorodibenzo-p-dioxin (TCDD)
                          740

-------
             PRIMARY ALUMINUM SUBCATEGORY
                                  SECT - VI
      54.
      69.
      70.
      86.
      87.
      89.
      90.
      91.
      92.
      93.
      94.
      95.
      96.
      97.
      98.
      99.
     100.
     101.
     102.
     103.
     104.
     105.
     109.
     110.
     111.
     112.
     113.
                          TABLE VI-3

           TOXIC POLLUTANTS NEVER FOUND ABOVE THEIR
                ANALYTICAL QUANTIFICATION LEVEL
isophorone
di-n-octyl phthalate
diethyl phthalate
toluene
trichloroethylene
aldrin
dieldrin
chlordane
4,4'-DDT
4,4'-DDE
4,4'-ODD
alpha-endosulfan
beta-endosulfan
endosulfan sulfate
endrin
endrin aldehyde
heptachlor
heptachlor epoxide
alpha-BHC
beta-BHC
gamma-BHC
delta-BHC
PCB-1232
PCB-1248
PCB-1260
PCB-1016
toxaphene
(a)
(a)
(a)
(a)
(a)   Reported together as a combined value,
                               741

-------
              PRIMARY ALUMINUM SUBCATEGORY   SECT - VI
                           TABLE VI-4

     TOXIC POLLUTANTS DETECTED IN A SMALL NUMBER OF SOURCES

       4.  benzene
      20.  2-chloronaphthalene
      23.  chloroform
      42.  bis(2-chloroisopropyl) ether
      44.  methylene chloride
      62.  N-nitrosodiphenylamine
      65.  phenol
      66.  bis(2-ethylhexyl) phthalate
      67.  butyl benzyl phthalate
      68.  di-n-butyl phthalate
      74.  3,4-benzofluoranthene
      75.  benzo(k)fluoranthene
      77.  acenaphthylene
      83.  indeno(l,2,3-cd)pyrene
     106.  PCB-1242      (a)
     107.  PBC-1254      (a)
     108.  PCB-1221      (a)
     117.  beryllium
     126.  silver
     127.  thallium

(a)   Reported together as a combined value.
                              742

-------
              PRIMARY ALUMINUM SUBCATEGORY
SECT - VII
                            SECTION VII

                CONTROL AND TREATMENT TECHNOLOGIES
The   preceding   sections  of  this  supplement  discussed   the
wastewater sources, flows, and characteristics of the wastewaters
from  primary  aluminum  plants.   This  section  summarizes  the
description  of  these  wastewaters,   indicates  the  level   of
treatment  which  is currently practiced in the primary  aluminum
subcategory,  and  describes the treatment options considered  by
EPA for this subcategory.

TECHNICAL BASIS OF BPT

As  mentioned  in  Section  III,  EPA  promulgated  BPT  effluent
limitations   guidelines  for  the  primary   aluminum   smelting
subcategory  on  April 8,  1974.   In order to put the  treatment
practices  currently in place and the technologies  selected  for
BAT  options  into  the  proper perspective it  is  necessary  to
describe the technologies selected for BPT.   The BPT regulations
established by EPA limited the discharge of fluoride and TSS  and
required  the  control  of  pH.   The  best  practicable  control
treatment  currently available    identified was the treatment of
wet  scrubber  water  and  other  fluoride-containing   effluents
through  the precipitation of fluoride,  followed by settling  of
the  precipitate  and recycling of the clarified effluent to  the
wet   scrubbers.    Two  precipitation   technologies,   cryolite
precipitation  and  lime precipitation,  were  determined  to  be
effective  and  it was left to the individual operator to  select
the one best suited for his specific application.  Recycle of the
clarified effluent was required, but EPA recognized that complete
recycle  was  not practicable and made an allowance for  a  bleed
stream to be discharged.

CURRENT CONTROL AND TREATMENT PRACTICES

This  section  presents  a summary of the control  and  treatment
technologies  that are currently applied to each of  the  sources
generating  wastewater  in  this subcategory.   As  discussed  in
Section  V,  wastewater  associated  with  the  primary  aluminum
subcategory  is characterized by the presence of the toxic  metal
pollutants,  cyanide, toxic organics, fluoride, aluminum, oil and
grease,  and suspended solids.  Generally, these  pollutants  are
present  in  each of the waste streams  at  concentrations  above
treatability,  so these waste streams are commonly  combined  for
treatment  to  reduce  the concentrations  of  these  pollutants.
Construction  of  one wastewater treatment  system  for  combined
treatment,  in  some  instances, combines  streams  of  differing
alkalinity which reduces treatment chemical requirements.   Seven
plants  in  this subcategory currently have  combined  wastewater
treatment systems, eight plants operate lime and settle treatment
on at least a portion of their wastewater.  One plant operates  a
multimedia filter as an end-of-pipe polishing step.  Four options
                               743

-------
              PRIMARY ALUMINUM SUBCATEGORY
SECT - VII
were   considered  for  BAT,  BDT,  and  pretreatment   in   this
subcategory,  based  on combined treatment  of  these  compatible
wastewater streams.

ANODE AND CATHODE PASTE WET AIR POLLUTION CONTROL

Preparing anode paste requires  crushing,  screening,  calcining,
and grinding and mixing of coke and pitch.   These are inherently
dusty   operations   requiring  extensive  particulate   emission
controls.    Twenty-two  plants  preparing  paste  use  dry   air
pollution  control devices while only four use wet air  pollution
control  devices.   Three plants do not use any emission control.
Wastewaters associated with the wet air pollution control devices
have  treatable  concentrations  of  suspended  solids.   Organic
pollutants  such  as fluorene,  pyrene,  and  chrysene  that  are
evolved  during  calcining of the paste also occur  in  treatable
concentrations.  None  of the plants reporting this waste  stream
recycle  any  scrubber water.   Two of these plants use  chemical
precipitation  and sedimentation to treat  the  wastewater.   One
plant   uses  only  sedimentation,   while  the  remaining  plant
discharges without treatment.

ANODE BAKE PLANT WET AIR POLLUTION CONTROL

Anode  bake  plant  air emissions are  more  complex  than  paste
preparation  emissions  and  reportedly  are  more  difficult  to
control by dry methods.   This is due to the fact that bake plant
emissions contain combustion products,  volatilized hydrocarbons,
tars,  and  oils.   The fluorides present are introduced into the
bake  plant  as  cryolite when anode  butts  are  recycled.   Dry
electrostatic   precipitators   (ESP)  and  baghouses   may   not
adequately  control  fluorides since the tars  and  oils  emitted
cause  the  equipment to be susceptible to arcing  and  blinding,
respectively,  which  inhibit  the performance of these  systems.
Wet  control systems,  such as wet ESP or scrubbers,  are not  as
susceptible  to  problems caused by  tars  and  oils.   Fluidized
alumina  systems  are  dry systems which avoid the  tar  and  oil
blinding  and arcing problems previously mentioned.   Dry systems
are  used by 12 out of the 17 plants which control  anode  baking
emissions.   Three  plants use only baghouses,  three plants  use
activated alumina,  and two plants use both activated alumina and
baghouses.   Of  the five plants using wet control systems,  four
use wet scrubbers,  two use wet ESP, and two use dry ESP preceded
by wet scrubbers.

Wastewater from the wet air pollution control equipment at plants
where  anode  butts are recycled must be treated  for  fluorides,
tars, oils, and particulates.  If care is taken in the removal of
fused cryolite from the anode butts before reprocessing, fluoride
emissions  from the anode bake plant are greatly lowered;  hence,
the  fluoride concentrations in bake plant scrubber waters  would
be minimized.  Two of the five plants practice partial recycle of
the scrubber effluent (91 and 99 + percent).  Typical treatment of
this wastewater, practiced at all five plants, consists of alkali
addition  and  sedimentation for suspended  solids  and  fluoride
                               744

-------
              PRIMARY ALUMINUM SUBCATEGORY   SECT - VII
removal.

ANODE AND BRIQUETTE CONTACT COOLING

This wastewater is generated when green anodes and briquettes are
sprayed with water to accelerate their temperature loss and allow
faster handling.  Eleven of the 31 .plants in the primary aluminum
subcategory  reported  the  use  of  anode  contact  cooling  and
briquette  quenching water.   This wastewater contains  suspended
solids, fluoride, and organics.  One of the four plants reporting
this effluent practices 100 percent recycle,  thereby eliminating
its  discharge.   Another  plant utilizes anode cooling water  as
off-gas quench water in the bake plant.  All water is consumed by
evaporation,  thereby eliminating its discharge.  Alkali addition
and  sedimentation  can be used to remove  suspended  solids  and
fluoride.  The following treatment schemes are currently in place
in the industry:

     1.  No treatment - five plants,
     2.  Settling pond - one plant,
     3.  Alkali addition and sedimentation - one plant,
     4.  100 percent evaporation - two plants,
     5.  100 percent reuse in other plant processes - one plant,
     6.  Cooling tower, retention pond, recycle - one plant.

CATHODE REPROCESSING

Cathodes  are  reprocessed  to recover  cryolite  by  a  leaching
operation.   The cryolite  is then precipitated from the  leachate
and  reused.   The  supernatant from  the  precipitation  step  or
solids  underflow is the cathode reprocessing  wastewater.   Four
plants generate this wastewater.

As   discussed  in Section V,  wastewater from cathode  reprocessing
contains treatable concentrations of  suspended solids,  fluoride,
and  cyanide.    Its composition is similar to that of  the  potline
scrubber effluent,  and the treatment techniques used for potline
scrubber  water  are  used to  treat the  cathode   reprocessing
effluent.   The  pH  of  the cathode  reprocessing  wastewater  is
extremely alkaline  (pH of  approximately 11).   One plant reported
using  alkaline  chlorination to treat  cyanide prior to  discharge.
Three   plants  use cathode  reprocessing water as potline  scrubber
liquor  make-up.

POTLINE AND POTROOM WET AIR POLLUTION CONTROL

Wet  and dry emission control devices  are  used  to collect  potline
air  emissions  that contain particulates,  fluorides, hydrocarbons,
and   sulfur  oxides  immediately   above   the   electrolytic   cell.
Gaseous  fluorides  are  removed by  dry alumina adsorption or  wet
scrubbing,  while particulate collection  is  usually performed with
baghouses.

A typical  dry  potline  emission control system  includes hoods  and
ducts   to   collect  and  deliver  the gases from the  pots   to  air
                                745

-------
               PRIMARY ALUMINUM SUBCATEGORY   SECT - VII
 pollution  control  units (the first is  usually  a  cyclone-type
 device  to  separate coarse particulates),   a reactor section  in
 which  the  gases are contacted with the alumina,  and  a  fabric
 filter.   After passing through the fabric  filter,  the gases are
 released to the atmosphere.

 Activated alumina dry collection systems allow for the subsequent
 return of the alumina and sorbed fluoride compounds to the  pots.
 Generally  high  removal efficiencies for both  gaseous  fluoride
 compounds  and particulates  are obtained (e.g.,   greater than  99
 percent).   This  dry scrubbing process represents a  significant
 means  of reducing effluent  discharges at primary aluminum plants
 since it uses no water.

 Although  many  plants  have converted from wet   to  dry  primary
 scrubbing  since  1974,    nine  plants  still practice  wet  air
 pollution control for potline emissions.    One plant reporting  a
 potline  scrubber  uses  100  percent recycle of  this  wastewater.
 Five  other plants report partial  recycle ranging from 88 to  99+
 per cent.

 Potroom  emission  control systems handle larger  volumes  of  air
 than  potline  emissions  control  systems.    Because there  is  a
 larger volume of air  from this process,  dry scrubbing systems are
 very expensive.    A treated  baghouse  contains a  limited number of
 sites_for  adsorption;  therefore,   larger volumes of gas decrease
 the life of each filter  which in turn increases  operating  costs.
 Consequently,  plants  have typically used  wet scrubbing systems to
 control  potroom emissions.    Seven plants  use secondary emission
 controls  (i.e.,   potroom emission control)  consisting  of  spray
 chambers  or   packed   towers.    One  plant   reported  using   foam
 scrubbers.    Six  plants with potroom scrubbers  reported  partial
 recycle rates  of scrubber  water  ranging from 42  to 99+ percent.

 Water from wet scrubbers will  contain fluoride, metals,  suspended
 solids,  and   organics in  treatable concentrations and is  treated
 to   remove   impurities before  it is recycled.    In  the   case   of
 primary potline  and secondary  potroom wet scrubbers,  the  fluoride
 dissolved   in  the  water  is  precipitated   and   settled.   This
 treatment  also reduces the suspended  solids  and metals content  at
 the  same time.

 The method most  commonly used  to remove the  fluoride  from  wet  air
 pollution  control  wastewaters  from potlines  and   potrooms   is
 precipitation  either as  cryolite or as calcium fluoride.   In  the
 first   case,   sodium  aluminate  (or  caustic   soda   and  hydrated
 alumina) is added.  In the second  case, a lime slurry  (or  calcium
 chloride)  is used.   After precipitation, the  slurry  is  sent to a
 thickener.   The  treatment  of  wet  scrubber  liquor   to   recover
 cryolite  results  in sufficient removal of    fluoride  to  permit
 recycle  of  the treated liquor.    The process also  recovers   the
 fluoride  in   a form which can be  returned to  the  aluminum  cell
bath.   The value of the recovered  cryolite  partially offsets  the
cost of the treatment process.   However,  the gradual buildup of
pollutants in  the scrubber liquor  requires a blowdown, preventing
                               746

-------
              PRIMARY ALUMINUM SUBCATEGORY
SECT - VII
total recycle of scrubber liquor.   (Recovery of the cryolite  is
practiced  at four of the nine plants reporting potline scrubbing
and by two of eight plants reporting potroom scrubbers.)

Elevated  levels  of  suspended solids (19 to  54,500  mg/1)  are
effectively   reduced   by   the   fluoride   precipitation   and
sedimentation process.

POT REPAIR AND POT SOAKING

Approximately  every two to three years the carbon liners of  the
electrolytic  cells  fail and must be  replaced.   To  facilitate
removal, the carbon liners are often soaked in water to make them
soft.   Reportedly,  some  plants use high pressure water jets to
remove the carbon liner.

Data on pot repair and pot soaking wastewater are  limited.   Two
of  the  plants reported in Table V-16 (page 688)  are  known  to
reuse  pot  repair-pot  soaking wastewater  as  potline  scrubber
liquor make-up, and one plant reported discharging its wastewater
to cathode reprocessing.  Two plants reported using  ion-exchange
to   reduce  cyanide  concentrations  and  lime  to   precipitate
fluoride.   Since  each primary aluminum plant must  replace  the
carbon liners (or cathodes) and very few plants report generating
or discharging this wastewater, it is assumed most plants recycle
and reuse pot soaking wastewater, or use dry removal techniques.

DEGASSING WET AIR POLLUTION CONTROL

The  method most commonly used for degassing and refining  molten
aluminum is to inject the aluminum with chlorine and other  inert
gases.   The hydrogen is absorbed into the chlorine bubbles,  and
gaseous  hydrochloric acid is subsequently produced.   Because of
the  corrosive nature of the gas stream,  it may be necessary  to
use  wet  air pollution control devices instead  of  dry  control
equipment  to  reduce  the pollutant  emissions.   Three  primary
aluminum plants reported using wet air' pollution controls for the
degassing operation.

Emphasis has been placed on examining methods for eliminating the
need  for wet control devices rather than on methods of  treating
the scrubber effluent.

Past  emission control efforts have resulted in  the  development
and successful use of gas mixtures such as chlorine plus an inert
gas,  or chlorine, carbon monoxide, and nitrogen.  In the case of
mixed gases,  gas burners or controlled combustion gas generators
are  used  to produce a gas of carefully controlled  composition.
The  following  is  a list of  alternative  in-line  fluxing  and
filtering methods:

     1.  Flotation with mixtures of chlorine and other gases,

     2.  Impingement, and
                               747

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               PRIMARY ALUMINUM  SUBCATEGORY
SECT - VII
      3.   Counter  flow  impingement.

 Since primary  aluminum plants are also often aluminum  formers,
 degassing  is  often performed in conjunction with  the  aluminum
 forming   demagging operation.   This can make the application  of
 alternative degassing  methods more difficult.   All of the  above
 listed  degassing alternatives are in commercial use on a regular
 basis and  may be considered established practice in one or  more
 producing  plants.   The viability of each degassing  alternative
 varies from plant to plant.   As a result,  the applicability  of
 any   specific process  alternative is determined on an  individual
 basis.

 CASTING CONTACT COOLING

 All of the  different aluminum casting contact cooling wastewaters
 are grouped together for discussion because they differ primarily
 in  the volume of water used and discharged.   With the exception
 of  oil and grease,  the pollutant concentrations in the  casting
 contact   cooling  waters are expected to  be  similar.   Oil  and
 grease  concentrations may differ among the wastewaters depending
 upon  the  use of lubrication agents for casting.

 Of the 31 primary aluminum plants, 28 reported the use of casting
 contact   cooling  water.   Three plants achieved  zero  discharge
 through   evaporation,  one plant achieved zero discharge  through
 spray irrigation,  and one achieved zero discharge by using  the
 contact   cooling  bleed stream as makeup water  for  the  potline
 scrubber.   The remaining plants discharge the cooling water.

 Casting   contact  cooling  water  will  contain  dissolved   and
 suspended  solids  and,  if  a mold lubricant is  used,  oil  and
 grease.   Control  of  wastewater from direct contact  cooling  is
 commonly  achieved by means of a cooling tower,  with recycle  of
 the   water.   A  bleed  stream  may  be  necessary   to   reduce
 concentrations  of  dissolved and suspended solids,  and oil  and
 grease.   Eleven  of the 28 plants recycle this  wastewater.   The
 recycle rates ranged from 20 to 99+ percent.

 Oil   and  grease  concentrations in the contact  cooling  effluent
 stream  may  be reduced by the use of oil  skimmers.   The  bleed
 stream  may  also  need  to be treated for  oil  and  grease  and
 dissolved and suspended solids.   Suspended solids may be removed
 simply    by  sedimentation,   while  dissolved  solids  must   be
 precipitated  from  solution.    Data  supplied  by  the  primary
 aluminum  subcategory indicate that three facilities  incorporate
 oil skimming into their wastewater treatment plants.

 CONTROL AND TREATMENT OPTIONS

 The Agency examined four control and treatment technology options
 between  proposal  and  promulgation that are applicable  to  the
primary   aluminum  subcategory.     The  options   selected   for
 evaluation  represent a combination of in-process flow reduction,
preliminary treatment technologies applicable to individual waste
                               748

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              PRIMARY ALUMINUM SUBCATEGORY   SECT - VII
streams, and end-of-pipe treatment technologies.

OPTION A

Option  A for the primary aluminum subcategory requires treatment
technologies  to  reduce the discharge of  pollutant  mass.   The
Option  A  treatment model consists of treatment   with  lime  and
settle (chemical precipitation and sedimentation)  applied to  all
waste   streams  and  oil  skimming,  where  required.   Chemical
precipitation  is  used  to remove metctls  and  fluoride  by  the
addition  of  lime followed by gravity  sedimentation.  Suspended
solids are also removed from the process.


OPTION B

Option  B  for the primary aluminum subcategory consists  of  all
treatment   requirements   of  Option  A   (lime    precipitation,
sedimentation,  and  oil  skimming) plus control  technologies  to
reduce   the   discharge  of  wastewater  volume    and   chemical
precipitation  with  ferrous  sulfate  to  control  cyanide  from
cathode  reprocessing wastewaters.   Water recycle and reuse  are
the principal control mechanisms for flow reduction.

EPA  considered cyanide treatment using chemical   oxidation  with
chlorine.   Although  the chlorine oxidation process can be  used
effectively for wastewater containing predominantly free cyanides
and  easily oxidizable cyanide complexes,  the Agency  determined
that  precipitation  with ferrous sulfate is more effective  than
chlorine  oxidation  for the removal  of  iron-cyanide  complexes
which are found in primary aluminum wastewater.

At  some  plants,  cathode reprocessing wastewater is  reused  in
potline wet air pollution control systems.  When this occurs, the
potline   scrubber  wastewater  will  exhibit  treatable  cyanide
concentrations  and  would require treatment for  cyanide  in  the
same manner as the cathode reprocessing wastewater.

OPTION C

Option  C  for the primary aluminum subcategory consists  of  all
control  and treatment requirements of Option B (in-process  flow
reduction,  oil  skimming,  cyanide  precipitation  with  ferrous
sulfate,  lime precipitation, and sedimentation), plus multimedia
filtration technology added at the end of the Option B  treatment
scheme.   Multimedia  filtration  is  used  to  remove  suspended
solids-, including precipitates of metals and fluoride, beyond the
concentration  attainable by gravity sedimentation.   The  filter
suggested  is of the gravity,  mixed media type,   although  other
forms  of filters such as rapid sand filters or pressure  filters
would also perform satisfactorily.   The addition of filters also
provides consistent removal during periods of time in which there
are  rapid  increases in flows or loadings of pollutants  to  the
treatment system.
                               749

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               PRIMARY ALUMINUM SUBCATEGORY   SECT - VII
 OPTION E

 Option  E for the primary aluminum subcategory consists of Option
 C (in-process flow reduction, oil skimming, cyanide precipitation
 with  ferrous sulfate,  lime  precipitation,  sedimentation,   and
 multimedia  filtration)  with the addition  of  activated  carbon
 adsorption  technology  at  the  end of the  Option  C  treatment
 scheme.   The  activated carbon process is used to  remove  toxic
 organic   pollutants  which  remain  after  lime   precipitation,
 sedimentation, and filtration.

 CONTROL AND TREATMENT OPTIONS REJECTED

 Three  additional control and treatment options  were  considered
 prior  to  proposing  mass limitations for  this  subcategory  as
 discussed  below.   Activated  alumina (fluoride adsorption)   and
 reverse  osmosis were rejected  because they are not  demonstrated
 in the nonferrous metals manufacturing point source category,  nor
 are  they clearly transferable.    Pretreatment of  certain waste
 streams  using  activated carbon was also   eliminated.    A pilot
 scale  treatability study performed by the Agency after   proposal
 demonstrated  that  toxic organic pollutants in primary   aluminum
 wastewaters are substantially removed through lime,   settle,   and
 filter treatment.  The findings  of this study eliminated   further
 consideration of activated carbon treatment.

 FLUORIDE TREATMENT EFFECTIVENESS ANALYSIS

 In settlement agreement negotiation,  the Agency re-evaluated   the
 variability   factors  for  fluoride   in   the  primary    aluminum
 subcategory  based  on petitioners claims  that   the   presence   of
 complex^fluoride ions and aluminum salts increase  the  difficulty
 of achieving  the  limitations  promulgated  in   June  1984.    The
 Agency  has   retained  the  long-term  mean   but   increased    the
 variability   factors   for  fluoride   to the  pooled  variability
 factors  computed  from data  for  seven  metal  pollutants   in   the
 combined  metals  data  base (4.10  and  1.82 for  the one  day   maximum
 and   the  monthly average of  daily values   variability   factors,
 respectively).   These   new  treatment   effectiveness  values   for
 fluoride  are   59.5 mg/1,  maximum  for any one day and  26.4  mg/1
 maximum monthly  average  of  daily values.
TREATMENT   EFFECTIVENESS  FOR  POTLINE  SCRUBBER
REPROCESSING WASTEWATERS
AND
CATHODE
The  Agency evaluated industry comments after proposal  and  made
additional  studies of the treatment effectiveness  of  treatment
technologies  applied to potline air pollution  control  scrubber
wastewater^  and cathode reprocessing wastewater.  These  studies,
reported  in  Section  V of this supplement,  indicate  that  the
nature of the wastewater matrix of these wastewaters is such that
treatment  effectiveness  values other than  those  displayed  in
Table  VII-21 of Vol 1 should be used. The Agency has elected  to
                               750

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              PRIMARY ALUMINUM SUBCATEGORY   SECT - VII
develop  mass  discharge  limitations for  these  two  wastewater
streams when they are uncomingled with any other waters based  on
the  results  of the special treatment studies.  These  treatment
effectiveness  values are summarized in Table VII-1  (page  735).
When  these  wastewaters  are comingled with  other  waters,  the
treatment effectiveness levels of Table VII-21, Vol 1  (page 248)
are used.

Spent  potliner  leachate may receive the  treatment  performance
values  developed for cathode reprocessing and provided: (a)  the
permit  writer  determines  on  a case by  case  basis  that  the
wastewater  matrices of cathode reprocessing and  spent  potliner
leachate  are comparable; and (b) the spent potliner leachate  is
not commingled with process or non-process wastewaters other than
cathode  reprocessing  or  potline  wet  air  pollution   control
operated in conjunction with cathode reprocessing. Spent potliner
leachate  resulting  from  atmospheric  precipitation  runoff  is
considered  a  site specific non-scope wastewater stream  by  the
Agency and for this reason specific limitations are not  provided
in this regulation.

BENZO(A)PYRENE TREATMENT EFFECTIVENESS ANALYSIS

In settlement negotiations after promulgation, the Agency revised
its  statistical analysis of benzo(a)pyrene data to  develop  one
day   maximum   and  monthly  average   treatment   effectiveness
concentrations as a basis for calculating mass discharge  limits.
The  recalculated  treatment  effectiveness  concentrations   are
0.0337  mg/1  maximum  for any one day and  0.0156  mg/1  maximum
monthly  average of daily values. The Agency also restricted  the
discharge  allowance  for benzo(a)pyrene to those  streams  which
actually contain this pollutant.
                               751

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               PRIMARY ALUMINUM SUBCATEGORY    SECT  - VII
                            TABLE  VII-1

       TREATMENT EFFECTIVENESS  FOR SELECTED  BUILDING BLOCKS
                 Lime  Settle and Filter  Technology
                              (mg/1)
Pollutant                Mean

 Acenaphthene            0.010
 Benzo(a)anthracene      0.023
*Benzo(a)pyrene          0.010

 3,4-Benzofluoranthene   0.010
 Benzo(k)fluoranthene    0.010
 Benzo(ghi)perylene      0.010

 Chrysene                0.023
 Dibenzo(a,h)anthracene  0.010
 Floranthene             0.114
 Pyrene                  0.079

*Antimony                2.99
*Cyanide                 1.1
*Nickel                  0.57

*Aluminum                1.9
*Pluoride              206
*TSS                    15
 One-day
 Maximum
  0.0337
  0.0337
  0.0337

  0.075
  0.0337
  0.384
  0.266

 12.0
  4.5
  2.3

  7.8
840
 61.5
 10-day
 Average
  0.0337   0.0156
  0.0775   0.036
  0.0337   0.0156
  0.0156
  0.0156
  0.0156

  0.036
  0.0156
  0.178
  0.123

  5.4
  2.0
  1.0
  3.5
380
 27.3
30-day
Average

   NC
   NC
   NC

   NC
   NC
   NC

   NC
   NC
   NC
   NC

   NC
   NC
   NC

   NC
   NC
   NC
*  = Regulated Pollutant
NC = Not calculated
NOTE:  These values may be used only for  calculating  allowances
for  cathode reprocessing and potline wet air  pollution  control
wastewaters   when  they  are  not  commingled  with  any   other
wastewaters.
                               752

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             PRIMARY ALUMINUM SUBCATEGORY   SECT - VIII




                           SECTION VIII

            COSTS, ENERGY,  AND NONWATER QUALITY ASPECTS
This  section describes the method used to develop the  estimated
costs  associated  with the control  and  treatment  technologies
discussed  in Section VII for wastewaters from  primary  aluminum
plants.   The  energy requirements of the considered  options  as
well as solid waste and air pollution aspects are also  discussed
in this section.

Section  VI  indicated that significant pollutants  or  pollutant
parameters  in  the  primary aluminum  subcategory  are  benzo(a)
pyrene,  aluminum,  antimony, nickel, cyanide, fluoride, TSS, pHf
and  oil and grease.   Metals and fluorides are most economically
removed by chemical precipitation,  sedimentation and filtration.
These   technologies  also  remove  toxic  polynuclear   aromatic
hydrocarbon's.   Cyanide concentrations can be reduced by chemical
precipitation with ferrous sulfate or by ion-exchange.  Activated
carbon is an effective treatment for removing organics.

LEVELS OF TREATMENT CONSIDERED

As  discussed in Section VII,  four control and treatment options
were considered for treating wastewater from the primary aluminum
subcategory.   Cost  estimates were developed for each  of  these
control  and treatment options.   Cost estimates,  in the form of
annual cost curves, have been developed for each of these control
and treatment options,  and they are presented in Section VIII of
the  General  Development Document.   The control  and  treatment
options  are  presented in Figures X-l through X-4 (pages  808
811) .

OPTION A

Option  A for the primary aluminum subcategory consists  of  lime
precipitation  and  sedimentation applied to combined  wastewater
streams.   Oil skimming is added as a preliminary treatment_  step
to remove oil and grease from all waste streams except stationary
and  shot  casting,  potline SO2 wet air pollution  control,   and
degassing wet air pollution control.

OPTION B

Option  B  for the primary aluminum subcategory consists  of  all
treatment   requirements   of  Option  A   (lime   precipitation,
sedimentation,  and  oil  skimming) plus control technologies_ to
reduce   the   discharge  of  wastewater  volume   and   chemical
precipitation  with  ferrous  sulfate  to  control  cyanide  from
cathode  reprocessing wastewaters.   Water recycle and reuse  are
the  principal  control  mechanisms  of  flow  reduction.    Flow
reduction  measures consist of recycle of contact  cooling  water
through  cooling  towers  and     recycle of  wet  air  pollution
                               753

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             PRIMARY ALUMINUM  SUBCATEGORY   SECT - VIII


control wastewater through holding tanks.

OPTION C

Option C consists of Option B  (cyanide precipitation  preliminary
treatment,  lime precipitation,  sedimentation,  oil skimming and
in-process  flow  reduction)   with  the  addition  of  multimedia
filtration added to the end of the Option B treatment scheme.

OPTION E

Option E consists of Option C  (lime precipitation, sedimentation,
oil   skimming,   in-process   flow  reduction,   and   multimedia
filtration)  with  the addition of  activated  carbon  adsorption
technology at the end of the Option C treatment scheme.

Cost Methodology

A  detailed  discussion of the methodology used  to  develop  the
compliance  costs has been presented.  Plant-by-plant  compliance
costs  have been estimated for the primary aluminum  subcategory.
The  total  costs  for the  final  primary  aluminum  subcategory
regulation are presented in Table VIII-1 (page 757).

The major general assumptions  used to develop  compliance  costs
have  been presented. Each subcategory contains a unique  set  of
waste streams requiring certain subcategory-specific  assumptions
to  develop compliance costs.  Six major  assumptions  applicable
specifically  to the primary aluminum subcaategory are  discussed
briefly below.

     (1)   Compliance costs for oil-water separation, flow reduc-
          tion via cooling towers,  and lime and settle are neces-
          sary to meet the previously promulgated BPT regulation
          for certain waste streams.   These costs are not
          included in the current compliance costs if the treat-
          ment is in place and of sufficient capacity,,   If
          additional capacity is required to treat waste streams
          not considered in the promulgated BPT regulation,  the
          cost for this capacity is included in the compliance
          cost estimate.

     (2)   In the consideration of activated carbon adsorption as
          an end-of-pipe technology,  each plant is analyzed  to
          determine whether separate  or  combined treatment of the
          organic bearing and organic free waste streams is
          economically justified.   The least costly configuration
          is then used to estimate  compliance costs.

     (3)   Sludge generated by lime  and settle treatment is
          assumed a hazardous waste when polynuclear aromatics
          are removed.

     (4)   Cyanide precipitation is  included as a preliminary
          treatment step on cyanide-bearing wastewaters only.
                               754

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             PRIMARY ALUMINUM SUBCATEGORY   SECT - VIII
          These waters originate only in cathode reprocessing
          facilities used by four plants.  Hazardous waste dis-
          posal costs were included for the sludges generated by
          cyanide precipitation.

     (5)  Capital and annual costs for plants discharging in both
          the primary and secondary aluminum subcategories are
          based on a combined treatment system and were appor-
          tioned to each subcategory on a flow-weighted basis.

     (6)  Capital and annual costs for plants discharging in the
          primary aluminum subcategory and another point source
          category are based on separate treatment systems since
          the respective regulations are based on different tech-
          nologies and control different pollutants.  Segregation
          costs are included to separate the wastewaters.

NONWATER QUALITY ASPECTS

Nonwater  quality  impacts  specific  to  the  primary   aluminum
subcategory,  including energy requirements,  solid waste and air
pollution are discussed below.

ENERGY REQUIREMENTS

The  methodology used for determining the energy requirements for
the  various  alternatives is discussed in Section  VIII  of  the
General   Development  Document.    Option  C,   which   includes
filtration, is estimated to consume five; percent more energy than
the  promulgated  BPT technology,  while activated  carbon  could
increase energy consumption by approximeitely 50 percent over BPT.
Option C in a typical plant represents cipproximately 0.2  percent
of  the total plant electrical requirements.   Therefore,  it  is
concluded  this regulation will have negligible effects on energy
consumption.

SOLID WASTE

Sludges  associated  with the primary aluminum  subcategory  will
necessarily  contain  toxic  quantities (and  concentrations)  of
toxic metal pollutants.  Wastes generated by primary smelters and
refiners are currently exempt from regulation by Act of  Congress
(Resource Conservation and Recovery Act (RCRA)), Section 3001(b),
as  presently interpreted by the Agency.   Consequently,  sludges
generated from treating industries' wastewater are not  presently
subject to regulation as hazardous wastes.

If  these wastes should eventually be identified or are listed as
hazardous,  they will come within the scope of RCRA's "cradle  to
grave"  hazardous waste management program,  requiring regulation
from the point of generation to point of final disposition. EPA's
generator   standards  would  require  generators  of   hazardous
nonferrous  metals manufacturing wastes to meet containerization,
labeling,  record keeping, and reporting requirements; if  plants
dispose of hazardous wastes off-site, they would have to  prepare
                               755

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             PRIMARY ALUMINUM SUBCATEGORY
SECT - VIII
a manifest which would track the movement of the wastes from  the
generator's premises to a permitted off-site treatment,  storage,
or  disposal   facility.  See 40 CFR 262.20 45 FR 33142  (May  19,
1980),  as  amended  at 45 FR 86973   (December  31,  1980).   The
transporter regulations require transporters of hazardous  wastes
to comply with the manifest system to assure that the wastes  are
delivered to a permitted facility.  See 40 CFR 263.20 45 FR 33151
(May  19, 1980), as amended at 45 FR 86973 (December  31,  1980).
Finally, RCRA  regulations establish standards for hazardous waste
treatment,  storage, and disposal facilities allowed  to  receive
such wastes.   See 40 CFR Part 464 46 FR 2802 (January 12,  1981),
47 FR 32274 (July 26, 1982).

Even if these  wastes are not identified as hazardous,  they still
must  be  disposed  of  in compliance with the  Subtitle  D  open
dumping standards,  implementing 4004 of RCRA.   See 44 FR  53438
(September 13,  1979).

Pilot-scale    work   performed  by  the  Agency  since   proposal
demonstrated    that   toxic  polynuclear   aromatic   hydrocarbon
pollutants  found in primary aluminum wastewaters  aire  removable
using  lime,   settle,  and filter technology.   As a result,  the
Agency  believes lime sludge from this subcategory will be  toxic
due to the presence of these organic contaminants.   In addition,
sludges generated during cyanide precipitation are ejxpected to be
hazardous under RCRA.  Consequently, in developing plant-by-plant
compliance costs for the primary aluminum subcategory, the Agency
considered  the  sludges generated as hazardous.   The  costs  of
hazardous   waste  disposal  were  considered  in  the   economic
analysis, and  they were determined to be economically achievable.
(This  is  a   conservative  assumption since  these  sludges  are
presently  subject to a statutory and regulatory  exemption  from
hazardous  waste status).   It is estimated that Options B and  C
will generate  approximately 730,000 tons/yr of waste sludge as 20
percent  solids.    Multimedia  filtration  technology  will  not
generate  any   significant amount of sludge over  that  resulting
from' lime precipitation and sedimentation.

AIR POLLUTION

There  is no reason to believe that any additional air  pollution
will  result from implementation of cyanide  precipitation,  lime
precipitation,  sedimentation,  filtration,  reverse osmosis, and
carbon  adsorption.  These  technologies transfer  pollutants  to
solid  waste   and  do  not involve air  stripping  or  any  other
physical process likely to transfer pollutants to air.   In those
plants  using   lubricants  for casting,  there  may  be  organics
present  in drift from cooling towers along with some particulate
matter used to  recycle casting contact cooling  water.   However,
the  Agency believes that the amount of organic constituents  and
particulate matter in the drift would not be significant.
                               756

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             PRIMARY ALUMINUM SUBCATEGORY   SECT - VIII
                          TABLE VIII-1

     COST OF COMPLIANCE FOR THE PRIMARY ALUMINUM SUBCATEGORY
                       DIRECT DISCHARGERS
                 (March 1982 Dollars,  Millions)
            Proposal Cost
Promulgation Cost
Option
A
B
C
D
Capital
11.1
33.9
38.3
47.4*
Annual
5.3
21.2
24.5
24.4*
Capital
7.5
14.5
16.0
26.2**
Annual
7.9
9.8
10.5
14.7**
* Activated carbon adsorption as a preliminary treatment.

** End-of-pipe carbon adsorption.
                               757

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PRIMARY ALUMINUM SUBCATEGORY   SECT - VIII
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                  758

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               PRIMARY ALUMINUM SUBCATEGORY   SECT - IX




                            SECTION IX

         BEST PRACTICABLE TECHNOLOGY CURRENTLY AVAILABLE
EPA   promulgated  BPT  limitations  for  the  primary   aluminum
subcategory  on  April 8,  1974 as Subpart B of 40 CFR Part  421.
Pollutants regulated by these limitations were fluoride, TSS, and
pH.  Unlike  the  current rulemaking,  the BPT  limitations  were
developed  for the entire aluminum smelting process,  not on  the
basis of individual wastewater streams.   EPA is not promulgating
any modifications to these limitations.

The following limitations establish the quantity of pollutants or
pollutant properties,  which may be discharged by a point  source
after  application  of  the best practicable  control  technology
currently available:
Pollutant or
Pollutant Property
Maximum for
Any One Day
  Maximum for
Monthly Average
                 Metric Units - kg/kkg of product
            English Units - lbs/1,000 Ibs of product
Fluoride
Total Suspended Solids
pH
   2.0             1.0
   3.0             1.5
Within the range of 6 to 9
       at all times
                               759

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PRIMARY ALUMINUM SUBCATEGORY
SECT - IX
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                760

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               PRIMARY ALUMINUM SUBCATEGORY
SECT - X
                             SECTION X

         BEST AVAILABLE TECHNOLOGY ECONOMICALLY ACHIEVABLE
The  effluent  limitations  are  based on the  best  control  and
treatment  technology used by a specific point source within  the
industrial category or subcategory,  or by another category where
it  is  readily transferable.  Emphasis is placed  on  additional
treatment techniques applied at the end of the treatment  systems
currently  used  for BPT,  as well as reduction of the amount  of
water  used  and  discharged,   process  control,  and  treatment
technology optimization.

The  factors  considered in assessing best  available  technology
economically  achievable (BAT) include the age of  equipment  and
facilities involved,  the process used, process changes, nonwater
quality  environmental  impacts (including energy  requirements),
and  the costs of application of such technology (Section  304(b)
(2)(B)  of  the  Clean  Water  Act).   BAT  represents  the  best
available technology economically achievable at plants of various
ages,  sizes,  processes,  or  other characteristics.   Where the
Agency  has  found  the  existing  performance  to  be  uniformly
inadequate,  BAT may be transferred from a different  subcategory
or  category.   BAT  may  include  feasible  process  changes  or
internal controls, even when not in common industry practice.

The  statutory assessment of BAT considers costs,  but  does  not
require  a balancing of costs against effluent reduction benefits
(see  Weyerhaueser vs Costle, 590 F. 2d 1011 (D.C.  Cir.  1978)).
However,  in  assessing the proposed BAT, the  Agency  has  given
substantial   weight  to  the  economic  achievability   of   the
technology.

TECHNICAL APPROACH TO BAT

In  pursuing,  this  second  round  of  effluent  limitations  and
standards, the Agency reviewed a wide range of technology options
and evaluated the available possibilities to ensure that the most
effective  and beneficial technologies were used as the basis  of
BAT.   To  accomplish this,  the Agency examined four  technology
alternatives prior to promulgating mass limitations,  which could
be applied to the primary aluminum subcategory as BAT options and
which  would  represent substantial progress toward reduction  of
pollutant discharges above and beyond progress achieved by BPT.

In summary, the treatment technologies considered for BAT are
presented below:

Option A  (Figure X-l, page 808) is based on

     o  Preliminary treatment with oil skimming  (where required)
     o  Chemical precipitation and sedimentation
                                761

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                PRIMARY ALUMINUM SUBCATEGORY   SECT - X
Option B  (Figure X-2, page 809) is based on

     o  Preliminary treatment with oil skimming  (where required)
     o  Preliminary treatment of cathode reprocessing wastewater
        with  ferrous sulfate precipitation
     o  Chemical precipitation and sedimentation
     o  In-process flow reduction of casting contact cooling
        water and scrubber liquor resulting from anode paste
        plants, anode bake plants, potlines, and potrooms

Option C  (Figure X-3, page 810) is based on

     o  Preliminary treatment with oil skimming  (where required)
     o  Preliminary treatment of cathode reprocessing wastewater
        with  ferrous sulfate precipitation
     o  Chemical precipitation and sedimentation
     o  In-process flow reduction of casting contact cooling
        water and scrubber liquor resulting from anode paste
        plants, anode bake plants, potlines, and potrooms
     o  Multimedia filtration

Option E  (Figure X-4, page 811) is based on

     o  Preliminary treatment with oil skimming  (where required)
     o  Preliminary treatment of cathode reprocessing wastewater
        with ferrous sulfate precipitation
     o  Chemical precipitation and sedimentation
     o  In-process flow reduction of casting contact cooling
        water and scrubber liquor resulting from anode paste
        plants, anode bake plants, potlines, and potrooms
     o  Multimedia filtration
     o  Activated carbon adsorption for toxic organic removal

The four options examined for BAT are discussed in greater detail
on the following pages.   The first option considered (Option  A)
is  analogous  to  the BPT treatment which was presented  in  the
previous section.

OPTION A

Option  A for the primary aluminum subcategory is  equivalent  to
the  treatment  technology that is the basis of  promulgated  BPT
effluent limitations.   The Option A treatment scheme consists of
preliminary  treatment  of casting contact cooling water  by  oil
skimming  and chemical precipitation and sedimentation applied to
the  combined  wastewater  discharges as  reported  in  the  data
collection portfolios.   Although oil and grease is a conventional
pollutant, oil skimming is needed for BAT to ensure proper metals
removal.    Oil  and grease interferes with the chemical  addition
and   mixing  required  for  chemical  precipitation   treatment.
Chemical precipitation is used to remove metals, toxic  organics,
and  fluoride  by  the  addition  of  lime  followed  by  gravity
sedimentation.   Suspended  solids  are  also  removed  from  the
process.
                               762

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               PRIMARY ALUMINUM SUBCATEGORY   SECT - X
OPTION B

Option  B  for the primary aluminum  subcategory  achieves  lower
pollutant  discharge  by  building upon the  Option  A  treatment
technology   of  oil  skimming,   chemical   precipitation,   and
sedimentation  (see  Figure  X-2,  page  783).   Option  B   uses
preliminary  cyanide precipitation technology to  reduce  cyanide
concentrations and flow reduction measures to reduce the quantity
of pollutants discharged.

Cyanide  precipitation,  based on ferrous sulfate  addition,  was
applied  only to wastewater generated from  cathode  reprocessing
and   potline  scrubber  liquor  when  cathode  reprocessing  was
performed  on-site.    At  some  plants,,   cathode   reprocessing
wastewater  is  reused  in  potline  wet  air  pollution  control
systems.   When this occurs,  the potline scrubber wastewater may
exhibit   treatable  cyanide  concentrations  and  would  require
treatment  for  cyanide  in  the  same  manner  as  the   cathode
reprocessing wastewater.  Ion exchange has been demonstrated on a
pilot scale in the primary aluminum industry.  Performance values
obtained  through  ion-exchange are very similar to those of  the
Agency's  pilot scale treatability study using  ferrous  sulfate.
Alkaline  chlorination of cyanide is demonstrated at one  primary
aluminum plant.

Flow reduction measures,  including in-process changes, result in
the  elimination of some wastewater streams and the concentration
of pollutants in other effluents.  As explained in Section VII of
the   General   Development  Document,   treatment  of   a   more
concentrated  effluent  allows  achievement  of  a  greater   net
pollutant  removal and introduces the possible economic  benefits
associated  with treating a lower volume of wastewater.   Methods
used  in   Option B to reduce process wastewater  generation  and
discharge rates are discussed on the following page.

Recycle  of  Anode  and Casting  Contact  Cooling  Water  Through
Cooling Towers

The  cooling and recycle of contact cooling water is practiced by
22 of the 31 plants reporting this wastewater.   The function  of
contact  cooling  water is to quickly remove heat from the  newly
formed  anode  or  cast  aluminum.    Therefore,   the  principal
requirements  of  the water are that it be cool and  not  contain
dissolved solids at a concentration that would cause water  marks
or  other surface imperfections.   There is sufficient experience
within the nonferrous metals manufacturing category with  contact
cooling wastewater to assure the success of this technology using
cooling  towers  or heat exchangers (refer to Section VII of  the
General  Development Document).   Although one plant reported  it
did not discharge any anode quench water by reason of 100 percent
recycle,  a blowdown or periodic cleaning is needed to prevent  a
buildup  of dissolved and suspended solids.   (EPA has determined
that  a blowdown of 10 percent of the water applied in a  process
is adequate.)
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               PRIMARY ALUMINUM SUBCATEGORY   SECT - X
Recycle of Water Used in Wet Air Pollution Control

There  are  six  wastewater  sources  associated  with  wet   air
pollution  control  which  are  regulated  under  these  effluent
limitations:

     1.  Anode paste plant,
     2.  Anode bake plant,
     3.  Potline,
     4.  Potline SC-2,
     5.  Potroom, and
     6.  Degassing.

Table  X-l  (page 782) presents the number  of  plants  reporting
wastewater   use  with  these  sources,  the  number  of   plants
practicing recycle of scrubber liquor, and the range of  recycle.
The water scrubs particulate matter and fumes from the emissions,
requiring  a blowdown or periodic cleaning of scrubber liquor  to
prevent the buildup of dissolved and suspended solids.
skimming,
considered
technology
filtration
OPTION C

Option  C for the primary aluminum subcategory builds upon Option
B  by adding multimedia filtration technology to the end  of  the
in-process flow reduction, lime precipitation, sedimentation, oil
            and   cyanide  precipitation  with  ferrous  sulfate,
            for  Option  B.    A  schematic  of  this   treatment
            is  presented in Figure X-3  (page  784)   Multimedia
             is  used  to  remove  suspended  solids,   including
precipitates  of  metals and fluoride, beyond  the  concentration
attainable  by gravity sedimentation. The filter suggested is  of
the  gravity, mixed media type, although other forms of  filters,
such  as  rapid  sand filters or  pressure  filters,  would  also
perform satisfactorily.

OPTION E

Option  E  for the primary aluminum subcategory consists  of  in-
process flow reduction,  lime precipitation,  sedimentation,  oil
skimming,   cyanide  precipitation  with  ferrous  sulfate,   and
multimedia  filtration,  with  the addition of  activated  carbon
adsorption  technology.   The activated carbon process is used to
increase the removal of toxic organics after lime  precipitation,
sedimentation, and filtration.

INDUSTRY COST AND POLLUTANT REMOVAL ESTIMATES

As one means of evaluating each technology option,  EPA developed
estimates  of  the pollutant reduction and the  compliance  costs
associated with each option.   The methodologies are described on
the following page.

POLLUTANT REMOVAL ESTIMATES
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               PRIMARY ALUMINUM SUBCATEGORY   SECT - X
A  complete description of the methodology used to calculate  the
estimated  pollutant reduction achieved, by the application of the
various  treatment  options  is presented in  Section  X  of  the
General  Development  Document.   The  data used  for  estimating
pollutant  removals  are  the same as those used  to  revise  the
compliance costs.

Sampling  data collected during the field sampling  program  were
used  to  characterize  the major waste  streams  considered  for
Simulation?   At  each sampled facility,  the sampling data  were
production  normalized  for  each unit operation  (i.e.,  mass  of
pollutant  generated  per mass of  product  manufactured).   This
value,       referred to as the raw waste,  was used to  estimate
the  mass  of  toxic  pollutants  generated  within  the  primary
aluminum   subcategory.    By  multiplying  the   total   indu^try
production for a unit operation times the corresponding raw waste
SaluS,  the  mass of pollutant generated for that unit  operation
was estimated.

The volume of wastewater discharged after the application of each
treatment  option was estimated for each operation at each  plant
by  comparing the actual discharge to the regulatory  flow.   The
smaller  of the  two values was selected and summed with the other
plant  flows.  The mass of pollutant discharged was then estimated
by multiplying the achievable  concentration values attainable  by
the  option  (mg/1) by the estimated volume of process  wastewater
discharged by the  subcategory.    The mass of pollutant removed is
the  difference  between  the  estimated mass of pollutant generated
within the subcategory and the mass of pollutant  discharged after
application of the  treatment option.

The pollutant removal  estimates  for  the  direct dischargers  in  the
primary  aluminum  subcategory are presented  in Tables X-2   (page
783)   through X-5 (page  786).  Table X-2  shows  the   removals   for
the  toxic organic pollutants.  For inorganic  pollutants,   removal
estimates were   determined  based on   the  long-term  achievable
concentration  values  from either the  combined metals  data  base
 (CmT)  or an alternate  data base developed  from  the  pilot-scale
 ireatability study (see  Section  VII).   Treatment  performance data
 gathered  during ?he pilot-scale study demonstrated  that  plants
 operating   cathode   reprocessing  operations   and   using   the
 wKtJwatlr  as makeup for potline scrubber liquor cannot  achieve
 the  performance values  proposed for antimony,  nickel,   aluminum,
 fluoride,  and   total  suspended  solids.  Therefore,    alternate
 treatment  performance values from the study (Table  VI1-1,  page
 752)   were used to estimate  pollutant removals for those  primary
 aluminum  plants that operate cathode reprocessing and  commingle
 the  resulting   wastewater with potline  scrubber  ljj£'-   <™»e
 treatment  performance  is discussed in  greater  detail  below.)
 Pollutant  removal  estimates for plants that  do  not  commingle
 cathode reprocessing wastewater and potline scrubber liquor  were
 calculated using thl CMDB based treatment effectiveness values in
 Table"  VI1-21 (Vol-1 page 248).   Tables X-3 and X-4  Present  the
 inorganic  pollutant  removal  estimates  using  the  CMDB  based
                                765

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                PRIMARY ALUMINUM SUBCATEGORY   SECT - X
 treatment effectiveness and the alternate treatment effectiveness
 values in Table VII-1, respectively.  Inorganic pollutant removal
 totals for all direct dischargers are presented in Table X-5.

 COMPLIANCE COSTS

 Compliance costs presented at proposal were estimated using  cost
 curves,  _which   related   the  total  costs   associated   with
 installation  and operation of wastewater treatment  technologies
 to plant process wastewater discharge.   EPA applied these curves
 on  a  per  plant  basis,  a  plant's  costs—both  capital,   and
 operating  and maintenance—being determined by what treatment it
 has  in place and by its individual process wastewater  discharge
 (from  dcp).  The final step was to annualize the capital  costs,
 and  to sum the annualized capital costs,  and the operating   and
 maintenance  costs,   yielding  the  cost of  compliance  for   the
 subcategory.  Since  proposal, the cost estimation methodology was
 changed  as discussed in Section VIII of this document.  A design
 model  and  plant  specific  information  were  used  to  size  a
 wastewater  treatment system for each discharging facility.  After
 completion of the design, capital and annual costs were estimated
 for each unit of the wastewater treatment system.    Capital costs
 were developed from  vendor quotes and annual costs were developed
 from literature.   The revised compliance costs are presented  in
 Table VIII-1 (page 757).

 BAT OPTION  SELECTION

 EPA's  proposed  BAT  was  based  on  lime,   settle,   and  filter
 technology   and flow reduction,   with preliminary   treatment   for
 organics  and cyanide using activated carbon and ferrous   sulfate
 precipitation,  respectively.   Numerous comments were  received  on
 the  proposed  technology stating,  among  other  things,,   that   the
 Agency did  not  account  for  the removal of  toxic organics  in   lime
 and settle  treatment.   The  transfer  of cyanide  precipitation   and
 associated  performance  values  was  also contested as   unachievable
 on   primary  aluminum wastewaters.   The Agency   performed pilot-
 scale work  on potline scrubber  blowdown and  cathode   reprocessing
 wastewater  at a primary aluminum facility  following proposal  (see
 Sections  V and VII).  Analytical  data gathered during  the  study
 indicate  toxic   organic  pollutants  present  in   primary   aluminum
 wastewaters  are controllable  through  lime, settle, and multimedia
 filtration  treatment  technology.   The  toxic  organics, present  as
 polynuclear   aromatic hydrocarbons,  are only  slightly soluble  in
 water, and  thus are treatable  using  sedimentation and   filtration
 techniques. Removals  by this technology exceed  99 percent of  all
 toxic  organics  present.   In addition, the most  toxic  of  the
 polynuclear  aromatic  hydrocarbons,   including  the   carcinogen
 benzo(a)pyrene,  are  removed  to the limit of  quantification  by
 this   technology. For these reasons, the Agency does not  believe
 it is warranted to include the use of activated carbon to  remove
 the  small  amounts  of these  less  toxic  polynuclear  aromatic
hydrocarbons  remaining after  application of lime,  settle,  and
filtration  technology.   At-the-source  limitations  for   toxic
organic pollutants are not appropriate because toxic organics  are
                               766

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               PRIMARY ALUMINUM SUBCATEGORY   SECT - X


effectively controlled with lime, settle, and filter treatment.

Thus,  the  promulgated  BAT  mass limitations  for  the  primary,
aluminum subcategory are based on end-of-pipe lime precipitation,
sedimentation, and multimedia filtration.  Preliminary  treatment
of   cyanide  is  based  on  cyanide  precipitation.    Treatment
effectiveness values for toxic organic pollutants and for certain
toxic  metals (Table VII-1) are based on data from  the  Agency's
pilot plant study. They apply to potline wet scrubber and cathode
reprocessing  wastewaters  provided  these  wastewaters  are  not
commingled  with any other waters (see below).   In-process  flow
reduction  of scrubber liquors and contact cooling water  through
recycle is also included.

Data   gathered  through  specific data,  requests   show   cathode
reprocessing  wastewaters  are normally  used as potline  scrubber
liquor   make-up.    An  at-the-source   limit  for  cyanide   was
considered  to  prevent dilution of potline  scrubber  liquor  or
cathode reprocessing as a means of compliance.   An at-the-source
limit  would  be  appropriate if there were a risk  that  cyanide
could  be  diluted to below levels detectable at the end  of   the
pipe  as a result of mixing with wastewaters that do not  contain
cyanide.   This  is not likely to occur  because the waste streams
containing cyanide,  cathode reprocessing wastewater, and potline
scrubber  wastewater have very high flows.   These streams  would
have  to be diluted at roughly a 100 to  one ratio for cyanide  to
be  undetected,   an  unlikely   result.,   Permit  writers  should
investigate,  however, whether this degree of dilution might occur
at  an  individual plant  (for example,   if storm water   is  being
centrally treated), in which case an at-the-source limit would be
needed to ensure treatment and removal of cyanide.

The   final regulation states that only the potline  wet  scrubber
and   cathode  reprocessing building blocks receive a cyanide  mass
limitation.   This effectively precludes dilution because it does
not make economic sense  for a plant to treat  its entire  flow when
it   can pretreat  these cyanide-containing streams.    (The  Agency
thus  developed compliance costs based on cyanide  pretreatment.)
In    addition,    a   mass  allowance  is provided  for   cathode
reprocessing   only   if   this  operation  is  not   conducted    in
conjunction   with   potline  wet   scrubbing.    Where   cathode
reprocessing   is  operated along with wet potline   scrubbing,   an
allowance   is provided only  for  the potline  scrubber  because only
a  single  flow  is associated with both operations.    In   essence,
the   flow   from   potline  scrubbing   is   routed   to   the cathode
reprocessing   operation   for  fluoride recovery,  and  then   routed
back  to  the  potline where a  blowdown  is  discharged.   There  is   no
independent  flow  from cathode  reprocessing.

FINAL AMENDMENTS  TO THE  REGULATION

For   the   Primary Aluminum  Subcategory,  EPA  promulgated   final
amendments   on  July   7,   1987  (52  FR 25552)   to  the  regulation
concerning  four  topics,  which are briefly described here.
                                767

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                PRIMARY ALUMINUM SUBCATEGORY   SECT - X
 EPA   amended   the  BAT  limitations  and  NSPS  and  PSNS   for
 benzo(a)pyrene in two manners:   first,  to incorporate variability
 factors  into the daily maximum and monthly average  limitations;
 and   second,   to   only  provide   discharge   allowances   for
 benzo(a)pyrene  to those processes which generate this substance.
 Further,   EPA  provided  clarification  on 2 items  pertaining   to
 regulation of benzo(a)pyrene.

 EPA amended the BAT limitations and NSPS and PSNS for fluoride to
 be based  upon the pooled variability factors calculated from data
 for  seven  metal  pollutants   in  the   CMDB,    instead  of   the
 variability  factors from the Electrical & Electronic  Components
 Phase II  regulation.

 EPA  provided brief guidance on the treatment  values  that  permit
 writers may provide for spent potliner  leachate,   even though  EPA
 considers spent potliner leachate to be non-process and therefore
 a  non-scope flow.

 EPA  has   amended the NSPS  pH standards for direct chill  casting
 contact cooling water to a  range of 6.0 to 10.0  standard units at
 all times.

 TREATMENT PERFORMANCE

 Overall treatment  performance for the cathode  reprocessing  waste
 stream,   as  well   as  treatment  performance  values  for  three
 specific  pollutants,  namely cyanide,  benzo(a)pyrene and fluoride,
 are discussed here with respect  to their  special  circumstances in
 the primary aluminum subcategory.

 Treatment   performance  data gathered  during the pilot-scale  study
 demonstrated    that   plants   operating    cathode    reprocessing
 operations  and using   the wastewater   as makeup  for   potline
 scrubber   liquor cannot achieve  the performance   values  proposed
 for  antimony,   nickel,   aluminum,   fluoride,  and total suspended
 solids. The Agency believes this  is due  to  the matrix differences
 resulting   from cathode reprocessing,.   The cathode   reprocessing
 wastewater, and subsequently the  potline  scrubber  liquor,  contain
 dissolved   solids   levels   in  the  five   to six  percent   range.
 Therefore,  the Agency is  promulgating separate  mass  limitations
 for   those   primary  aluminum  plants  that    operate   cathode
 reprocessing  and  commingle  resulting wastewater  with   potline
 scrubber liquor.   However,  to receive these  alternate  limitations
 the  plant  may not dilute  potline  scrubber  liquor   blowdown  or
 cathode  reprocessing   wastewater with any  process or   nonprocess
wastewater  source.    If  the potline scrubber blowdown  is   diluted
with other wastewaters,  the Agency believes  the complexity of  the
matrix  decreases  and   thus the  concentrations of  the  combined
metals   data   base  (as   well   as  the    transferred   antimony
concentration)  should be achieved.

In  fact,   a  statistical analysis of untreated  wastewater  data
shows  primary  aluminum  wastewater  to  be  significantly  less
contaminated  than  wastewater from the plants  in  the  combined
                               768

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               PRIMARY ALUMINUM SUBCATEGORY
SECT - X
metals data base.

The  variability  factors used to determine the mass  limitations
for   the  alternate  potline  scrubber  blowdown   and   cathode
reprocessing  are transferred from the combined metals data base.
The CMDB contains more data points than the pilot-scale study and
thus is a better source for determining variability for lime  and
settle treatment.

While  not  considered  a  process  wastewater  stream,  EPA  has
provided  guidance  to  permit  writing  authorities  that  spent
potliner  leachate,  resulting from either the stockpiling or the
landfilling  of spent potliners,  may also receive the  alternate
treatment  performance values developed for cathode  reprocessing
or  potline scrubber liquor commingled with cathode  reprocessing
wastewaters.   This guidance is appropriate if the permit  writer
determines  on a case-by-case basis that the wastewater  matrices
of   cathode   reprocessing  and  spent  potliner  leachate   are
comparable and the spent potliner leachate is not commingled with
process or nonprocess wastewaters other than cathode reprocessing
or potline wet air pollution control operated in conjunction with
cathode reprocessing.

The  Agency's  pilot-scale  treatment  performance  studies  also
revealed  performance  limits for cyanide precipitation  are  not
transferable  from coil  coating to primary  aluminum  wastewater.
The Agency believes the  cathode reprocessing operations discharge
much   higher  concentrations  of  cyanide than  observed  in  coil
coating   and impair treatment by  also  discharging extremely  high
dissolved solids  concentrations  (five  to  six  percent)  that
interfere with  precipitation   chemistry.   Therefore,  treatment
effectiveness   is  based  on the  Agency's pilot  study  of   these
wastewaters.    This  mean  was also  shown,  in data submitted by  a
primary   aluminum  facility,  to  be achievable   by  ion  exchange
technology  applied  to  cyanide-contaminated  groundwater.    _In
developing   variability   factors  for   cyanide   precipitation
technology,  the -mean variability  from  the combined metals  data
base   is  used because only two  data points were  generated  by  the
treatability study.

The   Agency  has  re-evaluated   the   treatment   performance    for
benzo(a)pyrene   and has  concluded that there  is  some   variability
 in  treatment of this  compound,  and that,  in  addition,  the  model
 treatment  technology,   lime,   settle and  filter  also  has   some
associated  operating  variability.  As such,  EPA has  changed  the
benzo(a)pyrene   effluent limitations  and standards  by  increasing
 the  daily maximum from 0.010 mg/1 to  0.0337 mg/1 and  by_adding  a
monthly  maximum average of 0.0156 mg/1.   These  limitations   were
 determined on  the basis  of a statistical analysis of  data  on  the
 treatability  of  benzo(a)pyrene  obtained  in  the  pilot  study
 referenced above.

 As a result of  these  changes,   the allowances for  benzo(a)pyrene
 are   only  applicable  to  those  processes   that  generate  it.
 Therefore,   no   discharge  allowance  will   be   provided   for
                                769

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                PRIMARY ALUMINUM SUBCATEGORY   SECT - X
 benzo(a)pyrene  in  the  degreasing wet  air  pollution  control,
 direct  chill casting contact cooling and continuous  rod  casting
 contact cooling building blocks.

 The  clarification  that EPA has  provided is twofold:    the   rule
 does  not mandate at-the-source limitations   for   benzo(a)pyrene,
 and  analytical  values at  or below the detection  limit  for   any
 EPA-approved  analytical method   will be counted  as   zeroes   for
 purposes of determining compliance.

 The   Agency   has  re-evaluated   lime  and    settle    technology
 performance   for  fluoride  removal.    The   proposed    treatment
 performance for fluoride was transferred from the  electrical   and
 electronic  component  manufacturing (phase  II) lime   and settle
 mean  performance.   Because of the presence  of complex  fluoride
 ions  and  aluminum  salts  in the  primary  aluminum   subcategory
 wastewaters,   petitioners to the  promulgated  regulation  claimed
 that  the fluoride limitations are not achievable.  EPA  is   thus
 retaining  the  long-term  mean but   increasing  the   variability
 factors for fluoride (49 FR 8751,  8757).   The revised  promulgated
 limitations   are  based on  the  pooled   variability   factors
 calculated  from data for seven metal  pollutants in the  combined
 metals data base.   The variability factors used are 4.10  and  1.82
 for  daily  and  monthly variability  factors,  respectively,  as
 opposed to the values 2.40  and 1.3 which  were used for  the  March
 1984 promulgation.   These new variability factors change  the  one-
 day and monthly treatment effectiveness values to those shown in
 Table   VII-21  (page  248,   Vol-l).For   the   primary    aluminum
 subcategory,  the one-day and monthly treatment effectiveness   for
 fluoride  become  59.5 and  26.4 mg/1,  respectively.    The  Agency
 believes  that  the  variability associated with the  metals   data
 will  more accurately represent the  fluoride  variability  in   this
 subcategory.

 WASTEWATER DISCHARGE RATES

 Important  production operations that precede  and follow reduction
 are   anode  paste preparation and  baking,  anode cooling,  cathode
 manufacturing,   and  degassing  and  casting of  molten aluminum.  At
 some  primary aluminum plants,  spent cathodes are reprocessed  to
 recover  cryolite.    All  of  these  operations are potential sources
 of wastewater  and are  evaluated to establish  effluent limitations
 for  the  primary  aluminum subcategory.

 Specific wastewater  streams  associated with the primary  aluminum
 subcategory  are  discharges  from  air pollution emission  control
 devices  for the paste  plant,  anode bake plant, potline, potroom,
 and   degassing and those  from green anode and  briquette  contact
 cooling,   casting contact cooling,  cathode reprocessing, and pot
 repair-pot  soaking.   Table  X-6  (page 787) lists the  production
 normalized wastewater  discharge rates allocated at BAT  for  these
wastewater  streams.   The  values  represent the  best  existing
practices of the subcategory,  as  determined  from the analysis of
data  collection portfolios and data gathered  through  comments.
                               770

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               PRIMARY ALUMINUM SUBCATEGORY   SECT - X
ANODE AND CATHODE PASTE PLANT WET AIR POLLUTION CONTROL
WASTEWATER

The  BAT  wastewater discharge rate at proposal for  anode  paste
plant   wet   air  pollution  control  was  103.0   1/kkg   (24.7
gallons/ton) of paste produced.  This rate was allocated for  the
users   of   wet  air  pollution  control  devices   to   control
particulates emanating from the handling of coke and pitch during
anode  paste  preparation.  Of the 29  plants  reporting  on-site
paste  preparation, 22 use dry control devices.  Four plants  use
water  scrubbers,  while one does not have any  emission  control
devices.  All of the plants with water scrubbers are once-through
dischargers.  The BAT discharge rate at proposal for this  stream
was based on 90 percent recycle or reuse of the average water use
of the four plants.

Data  submitted  through comments and gathered  through  specific
data  requests were used to re-evaluate the proposed anode  paste
plant  wet air pollution control flow allowance.  The  same  four
plants   considered  at  proposal  are  used  to  calculate   the
flow  allowance at primulgation.  The promulgated  BAT  discharge
rate  for this stream is based on 90 percent recycle or reuse  of
the  average  water  use  of the four  plants.   Using  the  data
presented  in  Table  V-l  (page  653)  the  flow  allowance   is
calculated as 136 1/kkg (33 gal/ton) of paste produced.

The  scope  of  this wastewater stream has  also  been  expanded.
After proposal, it was demonstrated to the Agency that  scrubbers
used  to control particulate and gaseous emissions  from  cathode
paste  plants are similar to anode paste plant  scrubbers.   Flow
and   production  relationships  between  these  operations   are
essentially identical.

ANODE BAKE PLANT WET AIR POLLUTION CONTROL WASTEWATER

The  BAT  wastewater discharge rate at proposal  for  anode  bake
plant wet air pollution control was 49.4 1/kkg (11.9 gallons/ton)
of  anode  baked.  The rate was allocated only for  those  plants
with  wet air pollution control devices.  Of the 19 anode  baking
operations  reported, eight plants were thought to use water  for
emission  control.  The BAT discharge rate used at  proposal  was
based on 90 percent recycle of the water used at two plants  with
the lowest water usage.

After  proposal,  numerous  data  were  received  by  the  Agency
indicating  that  baking  operations from plant to plant are  not
consistent  and  are fundamentally different.   As  described  in
Section  III,  three different types of anode bake  furnaces  are
used:  1) open top ring furnace, 2) closed top ring furnace,  and
3) tunnel kiln. Differences in the furnaces create different  air
pollution  control requirements due to variations in the  volumes
of  air  produced and organic  loadings.   Production  normalized
water discharge, scrubber type, and furnace type are presented in
                               771

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               PRIMARY ALUMINUM SUBCATEGORY   SECT - X
Table   V-3  (page  656).   As  shown,  water  discharge   varies
dramatically  with  furnace type and scrubber  type.   Therefore,
four different flow allowances are used for this waste stream:

     1.  Tunnel kilns (1,138 1/kkg, based on 90 percent recycle
         at plant 342);
     2.  Closed top ring furnaces (4,324 1/kkg, based on 90
         percent recycle at plant 343);
     3.  Open top ring furnaces with spray towers only (50 1/kkg,
         based on 90 percent recycle at plant 364); and
     4.  Open top ring furnaces with spray towers and wet
         electrostatic precipitators (730 1/kkg, based on actual
         discharge at plant 354).

Plant  371 operates a wet ESP and falls between allowances  three
and  four.   The  Agency believes allowance number four  is  more
appropriate  for  this plant since allowance number  three  would
require the plant to increase its recycle rate to 99+.  Plant 371
currently complies with allowance number four.

ANODE CONTACT COOLING AND BRIQUETTE QUENCHING WATER

The BAT discharge rate at proposal for the anode contact  cooling
waste stream was 621 1/kkg (149 gallons/ton) of anode cast.  This
was equivalent to 90 percent recycle at the two known discharging
plants  (based upon average water use).  Four of  the  thirty-one
primary  aluminum  facilities  were  thought  to  generate   this
wastewater stream.  Information on water discharged and  recycled
was not available for one of the four plants.  The two  remaining
plants  are direct dischargers and do not practice recycle.   The
fourth  plant  reported  100 percent  recycle  of  anode  contact
cooling  water.   Wastewater  rates considered  at  proposal  are
presented in Section V of this supplement.

Data  and  information collected through  comments  and  specific
requests  for  information  have been  used  to  re-evaluate  the
proposal  anode contact cooling flow allowance.  Many  commenters
requested the Agency provide a discharge allowance for  .briquette
quenching  since  it  is a similar  operation  to  anode  contact
cooling.   In both operations, unbaked anodes and briquettes  are
water  cooled to facilitate handling.  The  principal  difference
between the two is size. Production normalized water usage  rates
for  briquette  quenching compare favorably  with  anode  contact
cooling, and thus they are included in the flow allowance.  Table
V-5 (page 665) presents the production normalized discharge rates
for  the  11 plants known to use contact cooling  water  to  cool
anodes or briquettes.

Data  presented in Table V-5 indicate plants 345 and 349  use  an
inordinately  large volume of cooling water when compared to  the
other   production  normalized  water  usage   discharge   rates.
Excluding these two plants yields an average water usage of 2,090
1/kkg.   The promulgated BAT is based on 90 percent  recycle,  or
209 1/kkg (50 gal/ton).
                               772

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               PRIMARY ALUMINUM SUBCATEGORY
               SECT - X
CATHODE MANUFACTURING

EPA  has determined that this operation,  for which  a  discharge
allowance was proposed, does not exist.

At proposal, wastewater from cathode manufacturing was thought to
be the discharge from wet ball milling.   The Aluminum Association
has  supplied information and data to the Agency indicating  this
wastewater  source,  as  described, does not  exist.   For  those
plants listed in the supplemental development document with  this
wastewater  source,  the Aluminum Association has  presented  the
actual use of water in manufacturing cathode paste:
                Plant
                 340
                 346
                 349
                 365
 Water Use
Bearing cooling water

Bearing cooling water

Soaking of potliners

Cathode paste plant wet air
pollution control
Thus,  only  the  scrubber  liquor at plant 369  and  pot  repair
wastewater  at  plant  349  are  considered  process  wastewater.
Correspondence  with  the corporate office for plant  365  states
that plant 369 also has a scrubbing system for the manufacture of
cathode paste.

At  these  two plants coal-tar paste is manufactured to seal  the
seams  of pre-purchased cathodes.   During mixing of  the  paste,
hydrocarbons  are emitted and captured with wet scrubbers.   This
operation is very similar to anode paste manufacture and its  air
pollution  control systems.   Because the manufacture of  cathode
paste  is similar to manufacturing anode paste and the water usage
rates  are  similar,  the  anode paste plant  wet  air  pollution
control  allowance is redefined as anode and cathode paste  plant
wet air pollution control.

CATHODE REPROCESSING

The  BAT  wastewater  discharge  rate  at  proposal  for  cathode
reprocessing was 952  1/kkg  (228 gal/ton) of aluminum reduced from
electrolytic   reduction.  There  were five plants in the  primary
aluminum   subcategory   thought  to  generate   wastewater   when
reprocessing   cathodes.   None  of these  plants  reported   their
recycle  or  reuse  practices  for this  waste   stream.   The  BAT
discharge  allowance  was  determined  from an average of   the  five
reported  discharge   rates.  The discharge rates ranged   from 169
1/kkg  to 1480  1/kkg.

Data   gathered  through   specific data  requests   after   proposal
 indicate  the   flow allowance  required  for  cathode   reprocessing
wastewaters  was   overstated.   Plants  operating  potline   wet
                                773

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                PRIMARY ALUMINUM SUBCATEGORY   SECT - X


 scrubbers  and cathode reprocessing commingle the two streams  to
 recover  the  fluoride  as  cryolite.   Discharge  from  cryolite
 recovery  is  then  returned to the potline circuit and  used  as
 scrubber  liquor.  Thus,  the bleed from cathode reprocessing  is
 accomplished  with  the  potline scrubber  bleed.   There  is  no
 independent discharge from cathode reprocessing,  arid so the flow
 allowance  provided is for the potline  scrubber  bleed.   Plants
 with  cathode  reprocessing  were  included  in  determining  the
 potline  scrubber flow allowances.   A cathode reprocessing  flow
 allowance  is provided in the regulation,  but it only applies to
 those  plants operating dry potline scrubbers (and so  not  using
 cathode reprocessing bleed as makeup for wet scrubber).

 The  Agency has also changed the production normalizing  parameter
 for  cathode  reprocessing  from aluminum  produced  to   cryolite
 recovered.    In this way, a plant may obtain spent potliners from
 another facility and still be able to comply with the promulgated
 mass limitations.

 A  flow  allowance  of  35,028 1/kkg  of  cryolite  recovered  is
 selected for those plants operating cathode reprocessing and  dry
 potline scrubbers.  This flow allowance is currently demonstrated
 at  one primary aluminum facility using dry scrubbing.  This value
 was selected because the other three plants,  which reported  much
 larger  discharge  rates,  reuse  the  blowdown  in  the  potline
 scrubber circuit.

 POTLINE WET AIR POLLUTION CONTROL WASTEWATER

 The BAT wastewater discharge rate at proposal  for  the  potline air
 scrubbing  stream  was 838 1/kkg (201  gallons/ton)   of   aluminum
 produced from  electrolytic reduction.   Emissions   from  potline
 reduction  operations   are controlled by dry   or   wet  processes.
 Common dry  methods involve sorption of fluorine  gases  on  alumina
 followed by  fabric filtration  for particulate   removal.    Since
 1973,  ^  significant  progress  has   been  made   toward   effluent
 reduction through the  conversion of wet  emission  control  devices
 to   dry processes.   Of the 31  plants  surveyed at proposal,   there
 were   still   11 plants using wet processes, including  one   plant
 with   no discharge;  four  plants  using a  recirculation  or  recycle
 system,  with discharges  ranging  from 592  1/kkg  (142  gallons/ton)
 to   1,147   1/kkg   (277  gallons/ton);  and  6 plants   with   a   once-
 through  system   with  discharges ranging  from  20,210   1/kkg   (224
 gallons/ton)   to  59,200   1/kkg  (14,000   gallons/ton).     Zero
 discharge  at  one plant was  accomplished  by complete recycle  and
 reuse  of  treated  wastewater.   The proposed BAT discharge  rate for
 the  potline   air  scrubbing   system  was   based  on  the  average
 discharge rate of  the  four plants with recycle rates ranging  from
 91  to  99 percent.

After   proposing   the  flow allowance,  the Agency examined  water
usage   as it  relates to scrubber  type and  cell  technology.   No
obvious  trends   were  apparent,  so  the  flow allowance  was  not
adjusted.    In  addition,  no data  or  information  were   received
indicating   the production normalized flows used to calculate the
                               774

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               PRIMARY ALUMINUM SUBCATEGORY
SECT - X
flow   allowance  had  changed.    Therefore,   the  Agency   has
promulgated  the  flow allowance for potline  wet  air  pollution
control as proposed.

Data  and  information were received indicating that  two  plants
have  recently  installed  dry potline  scrubbing,  leaving  nine
plants with wet scrubbers.  Of these nine plants, two plants have
not reported sufficient data to determine water usage and recycle
practices.   Six plants have recycle rates ranging from 88 to 100
percent, while the last plant does not practice recycle.

POTLINE SO2 WET AIR POLLUTION CONTROL

A  flow  allowance has been added for scrubbers used  to  control
sulfur emissions from potlines.   Currently there are two  plants
operating scrubbers to control SO2 emissions from potlines, which
are  preceded  by  dry fluoride  scrubbers  using  alumina.   The
production normalized discharge rates for these two scrubbers are
1,430  1/kkg  (343  gal/ton)  and 1,250 1/kkg  (300  gal/ton)  of
aluminum  production.   Recycle rates are reported as 77  and  75
percent,  respectively.  The discharge allowance is based on  the
average of the two values:  1,340 1/kkg (321 gal/ton).

Sulfur dioxide in these two scrubbers is transferred from the gas
phase  to the liquid phase using sodium carbonate as a  scrubbing
medium.   Requiring 90 percent recycle for these two scrubbers is
not appropriate due to the intricate chemistry involved.   Sodium
scrubbers such as these are normally designed to operate at a TDS
level of five percent.   By convention, a sodium scrubbing system
is  considered to be operating in the concentrated mode when  the
TDS  concentration  in  the recirculation stream  is  about  five
percent.  The two plants in the primary aluminum subcategory with
sodium  scrubbers  operate at a TDS concentration of 10  percent.
Increasing the recycle rate at these two plants will  necessarily
increase  TDS which will affect scrubber performance.   At higher
recycle  rates,   mass  transfer  capabilities  are  reduced  and
equilibrium  within  the scrubber liquor  may  shift,  liberating
sulfur dioxide gas.

Makeup water is added to the scrubbing circuit to control the TDS
level.   Consequently,  blowdown  from the circuit  results  from
excess water in the system.

POTROOM WET AIR POLLUTION CONTROL WASTEWATER

The BAT wastewater discharge rate at proposal for the potroom air
scrubbing  stream was 1,305 1/kkg (314 gallons/ton)  of  aluminum
produced  from electrolytic reduction.  This rate  was  allocated
only  for  plants  using wet air pollution  control  devices  for
potroom emissions.  Of the 31 plants surveyed at proposal,  eight
practiced  potroom  emission  control either  to  supplement  the
potline  gas cleaning system or as the only means of  controlling
emissions from the reduction area.  All of these plants used some
form  of  wet  scrubbing.   Wastewater  discharge  rates   varied
considerably among these plants, ranging from 0 to 227,700  1/kkg
                               775

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               PRIMARY ALUMINUM SUBCATEGORY
SECT - X
 (54,600  gal/ton).  The dcp data  indicated that the  presence  of
 potline  scrubbing  is  not a factor contributing  to  the  large
 variations  of potroom scrubber water used and  discharged.   The
 proposed  BAT  discharge  rate was based on the  average  of  the
 discharge rates of the four plants with recycle systems.

 Additional  data  collected  and  received  after  proposing  the
 potroom scrubber flow allowance have been used to re-evaluate the
 allowance.  The Agency has learned that plant 349 reported  water
 usage  for experimental foam scrubbers.  Water usage of the  foam
 scrubber and spray towers are not expected to be similar; this is
 clearly demonstrated in the reported values.

 Updated  flow  and production data were also received for  plants
 359 and 360.   The new dcp submitted by these two plants indicate
 they  have  installed recycle systems and use  horizontal  tunnel
 roof scrubbers with spray systems.   However,  plant 360 uses  an
 inordinately  large  amount of scrubber liquor when  compared  to
 plant 359 and the other plants.   Discharge rates for potroom wet
 air pollution control are presented in Table V-12 (page 674). The
 promulgated discharge allowance is based on the average discharge
 rates  at  plants 354, 359, 364, and 353 adjusted to  90  percent
 recycle.  Thus, the flow allowance for potroom wet air  pollution
 control  is  1,660  1/kkg (398  gal/ton)  of  aluminum  reduction
 production.

 POT REPAIR AND POT SOAKING

 A  flow  allowance for pot repair and pot soaking water  was  not
 provided  in  the  proposed mass limitations because  the  Agency
 believed  this stream was site specific.   The Agency  has  given
 this   stream  further  attention,   however,   due  to  industry
 requesting a flow allowance.   Data gathered through Section  308
 requests  found  five plants discharging this  wastewater.   Data
 submitted  to support the Aluminum Association's report  entitled
 Aluminum  Industry  Wastewater  Survey indicates  a  sixth  plant
 discharges  this  waste stream.   A seventh plant has  also  been
 identified through information supplied in the dcp.   The  Agency
 believes  this  waste stream is present subcategory-wide  because
 each plant must repair pots and remove potliners (caithodes).  The
 complete recycle of this stream was reported by three plants. The
 belief  that this process can be operated with no  discharge  has
 been  confirmed  through conversations with  industry  personnel.
 Water  is  used primarily to soften the liner so thcit it  can  be
 removed.   The Agency is unaware of any water quality  restraints
 restricting the reuse of this water.  Therefore, a zero discharge
 allowance  is  established  for this waste stream  based  on  100
 percent reuse.


 DEGASSING WET AIR POLLUTION CONTROL

 No  BAT discharge allowance was provided for  degassing  scrubber
 wastewater in the proposed mass limitation.   The Agency believed
many  plants  had eliminated the need for degassing scrubbers  by
                               776

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               PRIMARY ALUMINUM SUBCATEGORY
SECT - X
using  alternative fluxing methods.    These  alternative  fluxing
methods  reduce  chlorine  fumes released in  the  operation  and
subsequently  eliminate  the need to remove fumes from  the  off-
gases to comply with opacity requirements.

However,  it  has been demonstrated to the Agency that  extensive
retrofits  would be required to install alternate in-line fluxing
and filtering.   Consequently,  the Agency has withdrawn the zero
discharge requirement and provided a discharge allowance based on
the average reported water usage rates.   The BAT discharge  rate
is 2,609 1/kkg (626 gal/ton) of aluminum refined.  Flow reduction
has  not been included for this stream due to the nature  of  the
fume being scrubbed.  Essentially, chlorine water will be  formed
and  recycle  methods reducing chlorine  concentrations  are  not
readily available.  Aeration could be used to reduce the chlorine
concentration prior to recycle; however, this would only transfer
the point source from one part of the plant to another.

DIRECT CHILL CASTING CONTACT COOLING

Direct  chill casting practices and the wastewater discharge from
this  operation are similar in the aluminum forming  and  primary
aluminum  reduction plants.   The data available do not  indicate
any  significant  difference in the amount of water required  for
direct  chill casting in a primary aluminum or  aluminum  forming
plant.    For   this  reason,   available  wastewater  data  were
considered together,  regardless of the affiliated  category,
establishing BAT effluent limitations.
                 in
In all, 27 primary aluminum plants and 61 aluminum forming plants
were  considered  to  have  direct chill  casting  operations  at
proposal.   Recycle  of the contact cooling water is practiced at
30 aluminum forming and 18 primary aluminum plants.  Of these, 12
plants  indicated  that  total recycle of  this  stream  made  it
possible  to  avoid any discharge  of  wastewater;  however,  the
majority  of the plants discharge a bleed stream.   The discharge
flow  for  this operation was based on the average of  the  best,
which was the average normalized discharge flow of the 29  plants
that  practice  recycle greater than 90 percent.   That flow  was
1,999  1/kkg (479 gal/ton) of aluminum product from direct  chill
casting.

Evaluation  of  the flow allowance user at  proposal  revealed  a
mistake in the calculation methodology.  A plant practicing  only
54   percent   recycle   was  inadvertently   included   in   the
determination  of  the flow rate.  In addition,  several  primary
aluminum  facilities were contacted to clarify dcp  responses  on
casting  methods.   Data from the aluminum  forming  and  primary
aluminum  facilities were pooled together and  those  discharging
plants  practicing  90 percent recycle or greater  (but  not  100
percent recycle) were averaged to determine the flow allowance of
1,329 1/kkg (319 gal/ton) of aluminum cast.
                                777

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                PRIMARY ALUMINUM SUBCATEGORY   SECT - X
 CONTINUOUS ROD CASTING CONTACT COOLING

 The  BAT  discharge  allowance at  proposal  for  continuous  rod
 casting  contact cooling stream was 104 1/kkg (25.0  gal/ton)   of
 aluminum  product  from rod casting.  This discharge flow  was  a
 reduction  of  the BPT discharge flow used  in  aluminum  forming
 based  on  primary  aluminum and aluminum  forming  plants  using
 recycle.  Two of the five primary aluminum plants thought to have
 continuous   rod  casting  reported  recycle,  one   plant   only
 periodically  discharges the stream, the other plant recycles   99
 percent.   Also,  17  aluminum forming plants,  which  recycle  a
 similar  type  of  cooling  stream  from  direct  chill  casting,
 reported recycle rates of 92 to nearly 100 percent.

 No information or data were received by the Agency after proposal
 indicating the flow allowance is inappropriate.    Therefore,  the
 continuous  rod  casting  flow allowance is  equivalent  to  that
 proposed.

 STATIONARY CASTING CONTACT COOLING

 In the stationary casting method,   molten aluminum is poured into
 cast iron  molds and generally allowed to air cool.    EPA is aware
 that spray quenching is used to quickly cool the molten  aluminum
 once cast  into the molds;   however,  the water is evaporated as it
 contacts  the  molten  metal.    As such,   there  is  no  basis  for
 providing  a pollutant discharge allowance.

 SHOT CASTING CONTACT COOLING

 Although  shot  manufacture  is not  prevalent   in  the  primary
 aluminum subcategory,  it  appears there is  one plant manufacturing
 shot.    The  BAT discharge  rate for  shot  casting is based on  the
 demonstrated water  use in  the  secondary aluminum subcategory.  The
 shot pasting  operation  in the primary aluminum subcategory   is
 identical   to  those   in   the   secondary   aluminum    subcategory.
 Therefore,  water  use  and discharge rates are  analogous.

 Through  specific information  requests  the Agency has  found  zero
 discharge   of  shot   casting cooling water  demonstrated  at   two
 secondary   aluminum   facilities (of  the  four   reporting   this
 operation).    Both  of  these  plants reported no product   quality
 constraints    due  to   100  percent   recycle.    Based    on    the
 demonstrated   zero  discharge   practices   for  shot  casting   the
 flow  allowance   requires zero  discharge  of   process  wastewater
 pollutants.

 REGULATED POLLUTANT PARAMETERS

 The  Agency placed particular  emphasis  on the  toxic  pollutants.
 The  raw wastewater concentrations  from  individual operations  and
 the  subcategory  as  a whole were   examined   to  select  certain
pollutants    and  pollutant  parameters  for   consideration   for
 limitation.   This  examination  and  evaluation,  presented   in
Section  VI,  concluded that 23 toxic pollutants are  present  in
                               778

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               PRIMARY ALUMINUM SUBCATEGORY   SECT - X
primary  aluminum  wastewaters  at  concentrations  that  can  be
effectively reduced by identified treatment technologies.

However,  the  cost  associated  with analysis  for  toxic  metal
pollutants has prompted EPA to develop an alternative method  for
regulating  and  monitoring toxic pollutant discharges  from  the
nonferrous metals manufacturing category.  Rather than developing
specific  effluent mass limitations and standards for each of the
toxic  metals  found  in  treatable  concentrations  in  the  raw
wastewater from a given subcategory,  the Agency is  promulgating
effluent  mass limitations only for those pollutants generated in
the  greatest  quantities  as  shown  by  the  pollutant  removal
estimates.   The pollutants selected for specific limitation  are
listed below:

     73.  benzo(a)pyrene
    114.  antimony
    121.  cyanide
    124.  nickel

By  establishing  limitations  and standards  for  certain  toxic
pollutants,  dischargers will attain the same degree  of  control
over toxic pollutants as they would have been required to achieve
had all the toxic pollutants been directly limited.

This  approach  is  justified  technically  since  the  treatment
performance   concentrations  used  for  lime  precipitation  and
sedimentation  technology  are based on optimized  treatment  for
concomitant  multiple metals removal.  Thus, even  though  metals
have  somewhat different theoretical solubilities, they  will  be
removed at very nearly the same rate in a lime precipitation  and
sedimentation  treatment  system  operated  for  multiple  metals
removal.  Filtration as part of the technology basis is  likewise
justified   because   this   technology   removes   metals   non-
preferentially.

The  performance  values used for toxic organic  pollutants  were
determined  in  pilot  scale treatability tests  performed  at  a
primary  aluminum- plant.   Data from the  study  indicate  toxic
organic  pollutants can be reduced to concentrations equal to  or
below the quantification limits for those pollutants.  The Agency
has selected benzo(a)pyrene as the only organic for limitation.

Benzo(a)pyrene  is  the  most toxic of the  polynuclear  aromatic
hydrocarbons  selected  in  Section  VI.    Each  toxic   organic
pollutant selected in Section VI was found removable in the pilot
scale  treatability  study using  lime,  settle,  and  filtration
treatment.   Therefore,  limiting benzo{a)pyrene will effectively
control  the other toxic organic pollutants present at  treatable
concentrations.   Those  pollutants effectively controlled by the
limitation of benzo(a)pyrene include:

     1.  acenaphthene
    39.  fluoranthene
    55.  naphthalene
                               779

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               PRIMARY ALUMINUM SUBCATEGORY   SECT - X
    72.  benzo(a)anthracene
    76.  chrysene
    78.  anthracene   (a)
    79.  benzo(ghi)perylene
    80.  fluorene
    81.  phenanthrene  (a)
    82.  dibenzo(a,h)anthracene
    84.  pyrene

        (a) — reported together

The  discharge allowance for benzo(a)pyrene applies only to those
processes   that  generate  it.    For  those   processes   where
benzo(a)pyrene  is not present,  no discharge allowance has  been
provided  for  benzo(a)pyrene.   This means that  in  calculating
effluent  limitations at the end of a  combined treatment system,
no  allowance  for  benzo(a)pyrene  may  be  included  for  these
processes.   In addition, monitoring of benzo(a)pyrerie from these
processes  (at-the-source)  will  not  be   required.    However,
monitoring  could be required at the discretion of the permitting
or  control  authority.   EPA has also  amended  the  specialized
definition  in  8421.21 to state that if a permittee  chooses  to
analyze  for  benzo(a)pyrene using any EPA - approved  analytical
method,  any non-detected values will be counted as zeros for the
purpose of determining compliance.   This approach is  consistent
with  the  methodology outlined in Section V for  developing  the
benzo(a)pyrene limitations.   The methodology used to develop the
limitations  treated the non-detected values from the pilot plant
study as zeros.  The detection limit for the approved EPA methods
of  GC/MS  and  gas  chromatography are  0.0025  and  0.01  mg/1,
respectively.

The  toxic metal pollutants selected for specific  limitation  in
the  primary  aluminum subcategory to control the  discharges  of
toxic metal pollutants are antimony and nickel.   Cyanide is also
selected  for  limitation  since  the  methods  used  to  control
antimony  and nickel are not effective in the control of cyanide.
The  following toxic pollutants are excluded from  limitation  on
the basis that they are effectively controlled by the limitations
developed for antimony and nickel:
   115.
   116.
   118.
   119.
   120.
   122.
   125.
   128.
arsenic
asbestos
cadmium
chromium
copper
lead
selenium
zinc
EFFLUENT LIMITATIONS

The   treatment   effectiveness  concentrations   achievable   by
application  of  the BAT treatment technology  are  discussed  in
Section  VII  of this supplement. The  achievable  concentrations
                                780

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               PRIMARY ALUMINUM SUBCATEGORY
SECT - X
(both one-day maximum and monthly average values)  are  multiplied
by  the BAT normalized  discharge,flows summarized in  Table  X-6
(page  787)  to calculate the mass of pollutants  allowed  to  be
discharged   per   mass  of  product.   The  results   of   these
calculations  in milligrams of pollutant per kilogram of  product
represent the BAT effluent limitations and are presented in Table
X-7 (page 789) for each individual waste stream.

Daily   maximum  and  monthly  average  treatment   effectiveness
concentrations  are provided for eleven toxic organic  and  seven
metallic  pollutants  that  are  effectively  controlled  by  the
control of benzo(a)pyrene, antimony and nickel. These values  are
displayed in Table VII-1 (page 752) for the convenience_of permit
writers.  While these pollutants are not specifically limited  by
the  primary aluminum limitations and standards,  permit  writers
may elect to include some or all of these pollutants in  specific
permits.
                                781

-------
                PRIMARY ALUMINUM  SUBCATEGORY   SECT - X
                            TABLE X-l
              CURRENT RECYCLE PRACTICES WITHIN THE
                  PRIMARY ALUMINUM SUBCATEGORY
                                   No. of Plants
                    No. of Plants   Practicing
                    With Wastewater  Recycle
Anode Paste Plant
Anode Bake Plant
Potline
Potroom
Degassing
4
5
9
8
4
0
2
6
6
0
                            Range of
                             Recycle
                            Values (%)
91 - 99
88 - 100
42 - 99
                              782

-------
             PRIMARY ALUMINUM  SUBCATEGORY
                                                SECT - X
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                    784

-------
PRIMARY ALUMINUM SUBCATEGORY
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                    785

-------
                PRIMARY  ALUMINUM SUBCATEGORY
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-------
             PRIMARY ALUMINUM  SUBCATEGORY
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-------
        PRIMARY ALUMINUM SUBCATEGORY
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-------
               PRIMARY ALUMINUM SUBCATEGORY
            SECT - X
                            TABLE X-7

  BAT EFFLUENT LIMITATIONS FOR THE PRIMARY ALUMINUM SUBCATEGORY


    Anode and Cathode Paste Plant Wet  Air. Pollution Control
Pollutant or Pollutant Property
Maximum for
Any One Day
  Maximum for
Monthly Average
            Metric Units - mg/kg of paste produced
       English Units - Ibs/million Ibs of paste produced
 Acenaphthene
 Benzo(a)anthracene
*Benzo(a)pyrene
 Benzo(ghi)perylene
 Chrysene
 Dibenzo(a,h)anthracene
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 Pyrene
*Aluminum
*Antimony
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 Chromium
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*Fluoride
 Lead
*Nickel
 Selenium
 Zinc

*Regulated Pollutant
     0.005
     0.011
     0.005
     0.005
     0.011
     0.005
     0.053
     0.036
     0.831
     0.262
     0.189
     0.027
     0.050
     0.174
     8.092
     0.038
     0.075
     0.112
     0.139
           0.002
           0.005
           0.002
           0.002
           0.005
           0.002
           0.025
           0.017
           0.369
           0.117
           0.084
           0.011
           0.020
           0.083
           3.590
           0.018
           0.050
           0.050
           0.057
                                789

-------
                •PRIMARY ALUMINUM SUBCATEGORY   SECT - X


                       TABLE X-7 (Continued)

   BAT EFFLUENT LIMITATIONS FOR THE PRIMARY ALUMINUM SUBCATEGORY
           Anode  Contact  Cooling and Briquette  Quenching


Pollutant  or  Pollutant Property
Maximum fo-r
Any One Day
  Maximum for
Monthly Average
               Metric Units  - mg/kg  of anodes cast
          English Units  -  Ibs/million Ibs of anodes cast
 Acenaphthene
 Benzo(a)anthracene
*Benzo(a)pyrene
 Benzo(ghi)perylene
 Chrysene
 Dibenzo(a,h)anthracene
 Fluoranthene
 Pyrene
*Aluminum
*Antimony
 Arsenic
 Cadmium
 Chromium
 Copper
*Fluoride
 Lead
*Nickel
 Selenium
 Zinc

*Regulated Pollutant
    0.007
    0.016
    0.007
    0.007
    0.016
    0.007
    0.082
    0.056
    1.277
    0.403
    0.291
    0.042
    0.077
    0.268
   12.440
    0.059
    0.115
    0.171
    0.213
          0.003
          0.007
          0.003
          0.003
          0.007
          0.003
          0.038
          0.026
          0.566
          0.180
          0.130
          0.017
          0.031
          0.127
          5.518
          0.027
          0.077
          0.077
          0.088
                               790

-------
               PRIMARY ALUMINUM SUBCATEGORY
           SECT - X
                      TABLE X-7 (Continued)

  BAT EFFLUENT LIMITATIONS FOR THE PRIMARY ALUMINUM SUBCATEGORY
      Anode Bake Plant Wet Air Pollution Control (Closed Top
                               Ring Furnace)
Pollutant or Pollutant Property
Maximum for
Any One Day
  Maximum for
Monthly Average
               Metric Units - mg/kg of anodes baked
          English Units - Ibs/million Ibs of anodes baked
 Acenaphthene
 Benzo(a)anthracene
*Benzo(a)pyrene
 Benzo(ghi)perylene
 Chrysene
 Dibenzo(a,h)anthracene
 Fluoranthene
 Pyrene
*Aluminum
*Antimony
 Arsenic
 Cadmium
 Chromium
 Copper
*Fluoride
 Lead
*Nickel
 Selenium
 Zinc

*Regulated Pollutant
    0.146
    0.335
    0.146
    0.146
    0.335
    0.146
    1.690
    1.151
   26.420
    8.345
    6.010
    0.865
    1.600
    5.535
  257.300
    1.211
    2.378
    3.546
    4.410
          0.067
          0.155
          0.067
          0.067
          0.155
          0.067
          0.782
          0.533
         11.720
          3.719
          2.681
          0.346
          0.349
          2.638
        114.200
          0.562
            ,600
1,
1,
            600
          1.816
                                791

-------
               PRIMARY ALUMINUM SUBCATEGORY   SECT - X


                      TABLE X-7 (Continued)

  BAT EFFLUENT LIMITATIONS FOR THE PRIMARY ALUMINUM SUBCATEGORY
       Anode Bake Plant Wet Air Pollution Control  (Open Top
               Ring Furnace With Spray Tower Only)
Pollutant or Pollutant Property
Maximum for
Any One Day
  Maximum for
Monthly Average
               Metric Units - mg/kg of anodes baked
         English Units - Ibs/million Ibs of anodes baked
 Acenaphthene
 Benzo(a)anthracene
*Benzo(a)pyrene
 Benzo(ghi)perylene
 Chrysene
 Dibenzo(a, h)anthracene
 Fluoranthene
 Pyrene
*Aluminum
*Antimony
 Arsenic
 Cadmium
 Chromium
 Copper
*Fluoride
 Lead
*Nickel
 Selenium
 Zinc

*Regulated Pollutant
    0.002
    0.004
    0.002
    0.002
    0.004
    0.002
    0.020
    0.013
    0.306
    0.097
    0.070
    0.010
    0.019
    0.064
    2.975
    0.014
    0.028
    0.041
    0.051
          0.001
          0.002
          0.001
          0.001
          0.002
          0.001
          0.009
          0.006
          0.136
          0.043
          0.031
          0.004
          0.008
          0.031
          1.320
          0.007
          0.019
          0.019
          0.021
                               792

-------
               PRIMARY ALUMINUM SUBCATEGORY
           SECT - X
                      TABLE X-7 (Continued)

  BAT EFFLUENT LIMITATIONS FOR THE PRIMARY ALUMINUM SUBCATEGORY
       Anode Bake Plant Wet Air Pollution Control (Open Top
       Ring Furnace With Wet Electrostatic Precipitator and
                           Spray Tower)
Pollutant or Pollutant Property
Maximum for
Any One Day
             Maximum for
           Monthly Average
               Metric Units - mg/kg of anodes baked
         English Units - Ibs/million Ibs of anodes baked
 Acenaphthene
 Benzo(a)anthracene
*Benzo (a) py r-ene
 Benzo(ghi)perylene
 Chrysene
 Dibenzo(a,h)anthracene
 Fluoranthene
 Pyrene
*Aluminum
*Antimony
 Arsenic
 Cadmium
 Chromium
 Copper
*Fluoride
 Lead
*Nickel
 Selenium
 Zinc

*Regulated Pollutant
    0.025
    0.057
    0.025
    0.025
    0.057
    0.025
    0.285
    0.194
      ,460
      409
    1.015
    0.146
    0.270
    0.934
   43.440
    0.204
    0.402
    0.599
    0.745
4,
1,
 0.011
 0.026
 0.011
 0.011
 0.026
 0.011
 0.132
 0.090
 1.978
 0.628
 0.453
 0.058
 0.110
 0.445
19.270
 0.095
 0.270
 0.270
 0.307
                               793

-------
               PRIMARY ALUMINUM SUBCATEGORY   SECT - X


                      TABLE X-7 (Continued)

  BAT EFFLUENT LIMITATIONS FOR THE PRIMARY ALUMINUM SUBCATEGORY


     Anode Bake Plant Wet Air Pollution Control (Tunnel Kiln)
Pollutant or Pollutant Property
Maximum for
Any One Day
  Maximum for
Monthly Average
               Metric Units - mg/kg of anodes baked
         English Units - Ibs/million Ibs of anodes baked
 Acenaphthene
 Benzo(a)anthracene
*Benzo(a)pyrene
 Benzo(ghi)perylene
 Chrysene
 Dibenzo(a,h)anthracene
 Fluoranthene
 Pyrene
*Aluminum
*Antimony
 Arsenic
 Cadmium
 Chromium
 Copper
*Fluoride
 Lead
*Nickel
 Selenium
 Zinc

*Regulated Pollutant
    0.038
    0.088
    0.038
    0.038
    0.088
    0.038
    0.445
    0.303
    6.953
    2.196
    1.582
    0.228
    0.421
    1.457
   67.710
    0.319
    0.626
    0.933
    1.161
          0.018
          0.041
          0.018
          0.018
          0.041
          0.018
          0.206
          0.140
          3.084
          0.979
          0.706
          0.091
          0.171
          0.694
         30.040
          0.148
          0.421
          0.421
          0.478
                               794

-------
               PRIMARY ALUMINUM SUBCATEGORY
           SECT - X
                      TABLE X-7 (Continued)

  BAT EFFLUENT LIMITATIONS FOR THE PRIMARY ALUMINUM SUBCATEGORY


    Cathode Reprocessing (Operated With Dry Potline Scrubbing
     and Not Commingled With Other Process or Nonprocess Waters)
Pollutant or Pollutant Property
Maximum  for
Any One  Day
           Maximum  for
         Monthly Average
           Metric Units - mg/kg of cryolyte recovered
      English Units - Ibs/million Ibs c>f cryolite recovered
 Acenaphthene
 Benzo(a)anthracene
*Benzo(a)pyrene
 Benzo(ghi)perylene
 Chrysene
 Dibenzo(a,h)anthracene
 Fluoranthene
 Pyrene
*Aluminum
*Antimony
 Arsenic
 Cadmium
 Chromium
 Copper
*Cyanide
*Fluoride
 Lead
*Nickel
 Selenium
 Zinc

*Regulated Pollutant
     1
     2
     1
     1
     2
     1
    13
     9
   273
   420
    48
     7
    12
    44
   157
29,430
     9
    80
    28
    35
.180
.715
.181
.180
.715
.180
.450
.326
.200
.400
.690
.006
.960
.840
.600
.000
.808
.570
.720
.730
    0.546
    1.257
    0.547
    0.546
    1.257
    0.546
    6.235
    4.317
  122.600
  189.200
   21.720
    2.802
    5.254
   21.370
   70.060
3,310.000
    4.554
   35.030
   12.960
   14.710
                                795

-------
                PRIMARY ALUMINUM SUBCATEGORY   SECT - X


                       TABLE X-7 (Continued)

   BAT EFFLUENT LIMITATIONS FOR THE PRIMARY ALUMINUM SUBCATEGORY


     Cathode  Reprocessing  (Operated With  Dry Potline Scrubbing
      and Commingled With  Other Process or  Nonprocess Waters)
 Pollutant  or  Pollutant  Property
Maximum for
Any One Day
  Maximum for
Monthly Average
            Metric Units - mg/kg of cryolite  recovered
      English Units -  Ibs/million  Ibs of cryolite  recovered
 Acenaphthene
 Benzo(a)anthracene
*Benzo(a)pyrene
 Benzo(ghi)perylene
 Chrysene
 Dibenzo(a,h)anthracene
 Fluoranthene
 Pyrene
*Aluminum
*Antimony
 Arsenic
 Cadmium
 Chromium
 Copper
*Cyanide
*Fluoride
 Lead
*Nickel
 Selenium
 Zinc

*Regulated Pollutant
    1.180
    2.715
    1.181
    1.180
    2.715
    1.180
   13.690
    9.326
  214.000
   67.610
   48.690
    7.006
   12.960
   44.840
  157.600
 2084.000
    9.808
   19.270
   28.720
   35.730
          0.546
          1.257
          0.547
          0.546
          1.257
          0.546
          6.339
          4.317
         94.930
         30.120
         21.720
          2.802
          5.254
         21.370
         70.060
        924.800
          4.554
         12.960
         12.960
         14.710
                               796

-------
               PRIMARY ALUMINUM SUBCATEGORY   SECT - X


                      TABLE X-7 (Continued)

  BAT EFFLUENT LIMITATIONS FOR THE PRIMARY ALUMINUM SUBCATEGORY


    Cathode Reprocessing (Operated With Wet Potline Scrubbing)
Pollutant or Pollutant Property
Maximum for
Any One Day
  Maximum for
Monthly Average
            Metric Units - mg/kg of cryolite recovered
      English Units - Ibs/million Ibs of cryolite recovered
 Acenaphthene
 Benzo(a)anthracene
*Benzo(a)pyrene
 Benzo(ghi Jgerylene
 Chrysene
 Dibenzo(a,h)anthracene
 Fluoranthene
 Pyrene
*Aluminum
*Antimony
 Arsenic
 Cadmium
 Chromium
 Copper
*Cyanide
*Fluoride
 Lead
*Nickel
 Selenium
 Zinc

*Regulated Pollutant
    0.000
    0.000
    0.000
    0.000
    0.000
    0.000
    0.000
    0.000
    0.000
    0.000
    0.000
    0.000
    0.000
    0.000
    0.000
    0.000
    0.000
    0.000
    0.000
    0.000
          0.000,
          0.000
          0.000
          0.000
          0.000
          0.000
          0.000
          0.000
          0.000
          0.000
          0.000
          0.000
          0.000
          0.000
          0.000
          0.000
          0.000
          0.000
          0.000
          0.000
                               797

-------
                PRIMARY ALUMINUM SUBCATEGORY   SECT - X


                       TABLE X-7 (Continued)

   BAT EFFLUENT LIMITATIONS FOR THE PRIMARY ALUMINUM SUBCATEGORY


    Potline Wet Air Pollution Control (Operated Without Cathode
                      Reprocessing)
 Pollutant or Pollutant  Property
Maximum for
Any One Day
  Maximum for
Monthly Average
   Metric  Units  -  mg/kg  of  aluminum  produced  from  electrolytic
                             reduction
     English  Units  -  Ibs/million  Ibs  of aluminum produced  from
                       electrolytic reduction
 Acenaphthene
 Benzo(a)anthracene
*Benzo(a)pyrene
 Benzo(ghi)perylene
 Chrysene
 Dibenzo(a,h)anthracene
 Fluoranthene
 Pyrene
*Aluminum
*Antimony
 Arsenic
 Cadmium
 Chromium
 Copper
*Fluoride
 Lead
*Nickel
 Selenium
 Zinc

*Regulated Pollutant
    0.028
    0.065
    0.028
    0.028
    0.065
    0.028
    0.328
    0.223
    5.120
    1.617
    1.165
    0.168
    0.310
    0.073
   49.860
    0.235
    0.461
    0.687
    0.855
          0.013
          0.030
          0.013
          0.013
          0.030
          0.013
          0.152
          0.103
          2.271
          0.721
          0.520
          0.067
          0.126
          0.511
         22.120
          0.109
          0.310
          0.310
          0.352
                               798

-------
               PRIMARY ALUMINUM SUBCATEGORY   SECT - X


                      TABLE X-7 (Continued)

  BAT EFFLUENT LIMITATIONS FOR THE PRIMARY ALUMINUM SUBCATEGORY
     Potline Wet Air Pollution Control (Operated With Cathode
      Reprocessing and not Commingled With Other Process or
                        Nonprocess Waters)
Pollutant or Pollutant Property
Maximum for
Any One Day
  Maximum for
Monthly Average
   Metric Units - mg/kg of aluminum produced from electrolytic
                            reduction
    English Units - Ibs/million Ibs of aluminum produced from
                      electrolytic reduction
 Acenaphthene
 Benzo(a)anthracene
*Benzo(a)pyrene
 Benzo(ghi)perylene
 Chrysene
 Dibenzo(a,h)anthracene
 Fluoranthene
 Pyrene
*Aluminum
*Antimony
 Arsenic
 Cadmium
 Chromium
 Copper
*Cyanide
*Fluoride
 Lead
*Nickel
 Selenium
 Zinc

*Regulated Pollutant
    0.028
    0.065
    0.028
    0.028
    0.065
    0.028
    0.328
    0.223
    5.120
   10.060
    1.165
    0.168
    0.310
    0.073
    3.771
  703.900
    0.235
    1.928
    0.687
    0.855
          0.013
          0.030
          0.013
          0.013
          0.030
          0.013
          0.152
          0.103
          2.271
          4.525
          0.520
          0.067
          0.126
          0.511
          1.676
        318.500
          0.109
          0.838
          0.310
          0.352
                               799

-------
                PRIMARY ALUMINUM SUBCATEGORY
           SECT - X
                       TABLE X-7 (Continued)

   BAT EFFLUENT LIMITATIONS FOR THE PRIMARY ALUMINUM SUBCATEGORY


      Potline Wet Air Pollution Control (Operated With Cathode
    Reprocessing and Commingled With Other Process or~Nonprocess
                            wastewaters)
 Pollutant or Pollutant Property
Maximum for
Any One Day
  Maximum for
Monthly Average
    Metric Units - mg/kg of aluminum produced from electrolytic
                             reduction
     English Units - Ibs/million Ibs of  aluminum produced from
                       electrolytic  reduction
  Acenaphthene
  Benzo(a)anthracene
 *Benzo(a)pyrene
  Benzo(ghi)perylene
  Chrysene
  Dibenzo(a,h)anthracene
  Fluoranthene
  Pyrene
 *Aluminum
 *Antimony
 Arsenic
 Cadmium
 Chromium
 Copper
*Cyanide
*Fluoride
 Lead
*Nickel
 Selenium
 Zinc

*Regulated Pollutant
    0.028
    0.065
    0.028
    0.028
    0.065
    0.028
    0.328
    0.223
    5.120
    1.618
    1.165
    0.168
    0.310
    0.073
    3.771
  49.860
    0.235
    0.461
    0.687
    0.855
          0.013
          0.030
          0.013
          0.013
          0.030
          0.013
          0.152
          0.103
          2.271
          0.721
          0.520
          0.067
          0.126
          0.511
          1.676
         22.130
          0.109
          0.310
          0.310
          0.352
                               800

-------
               PRIMARY ALUMINUM SUBCATEGORY
           SECT - X
                      TABLE X-7 (Continued)

  BAT EFFLUENT LIMITATIONS FOR THE PRIMARY ALUMINUM SUBCATEGORY


                Potroom Wet Air Pollution Control
Pollutant or Pollutant Property
Maximum for
Any One Day
              Maximum for
            Monthly Average
   Metric Units - mg/kg of aluminum produced from electrolytic
                            reduction
    English Units - Ibs/million Ibs of aluminum produced from
                      electrolytic reduction
 Acenaphthene
 Benzo(a)anthracene
*Benzo{a)py"rene
 Benzo(ghi)perylene
 Chrysene
 Dibenzo(a,h)anthracene
 Fluoranthene
 Pyrene
*Aluminum
*Antimony
 Arsenic
 Cadmium
 Chromium
 Coppe r
*Fluoride
 Lead
*Nickel
 Selenium
 Zinc

*Regulated Pollutant
    0.056
    0.129
    0.056
    0.056
    0.129
    0.056
    0.649
    0.442
   10.140
    3,
    2.
   204
   307
 0.332
 0.614
 2.125
98.770
 0.465
 0.913
 1.361
 1.693
0.026
0.060
0.026
0.026
0.060
0.026
0.300
0.205
  ,499
  ,428
  ,029
  ,133
4,
1,
1,
0,
                         0.249
                         1.013
                        43.820
                         0.216
                         0.614
                         0.614
                         0.697
                               801

-------
               PRIMARY ALUMINUM SUBCATEGORY   SECT - X


                      TABLE X-7 (Continued)

  BAT EFFLUENT LIMITATIONS FOR THE PRIMARY ALUMINUM SUBCATEGORY


        Potline SO? Emissions Wet Air Pollution Control
Pollutant or Pollutant Property
Maximum for
Any One Day
  Maximum for
Monthly Average
   Metric Units - mg/kg of aluminum produced from electrolytic
                            reduction
    English Units - Ibs/million Ibs of aluminum produced from
                      electrolytic reduction
 Acenaphthene
 Benzo(a)anthracene
*Benzo(a)pyrene
 Benzo(ghi)perylene
 Chrysene
 Dibenzo(a,h)anthracene
 Fluoranthene
 Pyrene
*Aluminum
*Antimony
 Arsenic
 Cadmium
 Chromium
 Copper
*Fluoride
 Lead
*Nickel
 Selenium
 Zinc

* Regulated Pollutants *
    0.045
    0.104
    0.045
    0.045
    0.104
    0.045
    0.524
    0.357
    8.194
    2.588
    1.864
    0.268
    0.496
    1.716
   79.790
    0.375
    0.738
    1.100
    1.368
          0.021
          0.048
          0.021
          0.021
          0.048
          0.021
          0.243
          0.165
          3.634
          1.153
          0.831
          0.107
          0.201
          0.818
         35.400
          0.174
          0.496
          0.496
          0.563
                               802

-------
               PRIMARY ALUMINUM SUBCATEGORY   SECT - X


                      TABLE X-7 (Continued)

  BAT EFFLUENT LIMITATIONS FOR THE PRIMARY ALUMINUM SUBCATEGORY


               Degassing Wet Air Pollution Control
Pollutant or Pollutant Property
Maximum for
Any One Day
  Maximum for
Monthly Average
   Metric Units - mg/kg of aluminum produced from electrolytic
                            reduction
    English Units - Ibs/million Ibs of aluminum produced from
                      electrolytic reduction
 Acenaphthene
 Benzo(a)anthracene
*Benzo(a)pyrene
 Benzo(ghi)perylene
 Chrysene
 Dibenzo(a,h)anthracene
 Fluoranthene
 Pyrene
*Aluminum
*Antimony
 Arsenic
 Cadmium
 Chromium
 Copper
*Fluoride
 Lead
*Nickel
 Selenium
 Zinc

*Regulated Pollutant
    0.088
    0.202
    0.088
    0.088
    0.202
    0.088
    1.020
    0.695
   15.940
    5.035
    3.627
    0.522
    0.965
    3.340
  155.200
    0.731
    1.435
    2.139
    2.661
          0.041
          0.094
          0.041
          0.041
          0.094
          0.041
          0.472
          0.322
          7.070
          2.244
          1.618
          0.209
          0.391
          1.591
         68.880
          0.339
          0.965
          0.965
          1.096
                               803

-------
               PRIMARY ALUMINUM SUBCATEGORY   SECT - X


                      TABLE X-7 (Continued)

  BAT EFFLUENT LIMITATIONS FOR THE PRIMARY ALUMINUM SUBCATEGORY


                    Pot Repair and Pot Soaking
Pollutant or Pollutant Property
Maximum for
Any One Day
  Maximum for
Monthly Average
   Metric Units - mg/kg of aluminum produced from electrolytic
                            reduction
    English Units - Ibs/million Ibs of aluminum produced from
                      electrolytic reduction
 Acenaphthene
 Benzo(a)anthracene
*Benzo(a)pyrene
 Benzo(ghi)perylene
 Chrysene
 Dibenzo(a,h)anthracene
 Fluoranthene
 Pyrene
*Aluminum
*Antimony
 Arsenic
 Cadmium
 Chromium
 Copper
*Fluoride
 Lead
*Nickel
 Selenium
 Zinc

^Regulated Pollutant
    0.000
    0.000
    0.000
    0.000
    0.000
    0.000
    0.000
    0.000
    0.000
    0.000
    0.000
    0.000
    0.000
    0.000
    0.000
    0.000
    0.000
    0.000
    0.000
          0.000
          0.000
          0.000
          0.000
          0.000
          0.000
          0.000
          0.000
          0.000
          0.000
          0.000
          0.000
          0.000
          0.000
          0.000
          0.000
          0.000
          0.000
          0.000
                               804

-------
               PRIMARY ALUMINUM SUBCATEGORY   SECT - X


                      TABLE X-7 (Continued)

  BAT EFFLUENT LIMITATIONS FOR THE PRIMARY ALUMINUM SUBCATEGORY


               Direct Chill Casting Contact Cooling
Pollutant or Pollutant Property
Maximum for
Any One Day
  Maximum for
Monthly Average
   Metric Units - mg/kg of aluminum product from direct chill
                             casting
     English Units - Ibs/million Ibs of aluminum product from
                       direct chill casting
 Acenaphthene
 Benzo(a)anthracene
*Benzo(a)pyrene
 Benzo(ghi)perylene
 Chrysene
 Dibenzo(a,h)anthracene
 Fluoranthene
 Phenanthrene
 Pyrene
*Aluminum
*Antimony
 Arsenic
 Cadmium
 Chromium
 Copper
*Fluoride
 Lead
*Nickel
 Selenium
 Zinc

*Regulated Pollutant
    0.045
    0.103
    0.045
    0.045
    0.103
    0.045
    0.520
    0.045
    0.354
    8.120
    2.565
    1.847
    0.266
    0.492
    1.701
   79.080
    0.372
    0.731
    1.090
    1.356
          0.021
          0.048
          0.021
          0.021
          0.048
          0.021
          0.240
          0.021
          0.164
          3.602
          1.143
          0.824
          0.106
          0.199
          0.811
         35.090
          0.173
          0.492
          0.492
          0.558
                               805

-------
                PRIMARY ALUMINUM  SUBCATEGORY   SECT - X


                      TABLE X-7  (Continued)

  BAT EFFLUENT  LIMITATIONS FOR THE PRIMARY ALUMINUM SUBCATEGORY


              Continuous Rod Casting Contact Cooling
Pollutant or Pollutant Property
Maximum for
Any One Day
  Maximum for
Monthly Average
    Metric Units - mg/kg of aluminum product from rod casting
   English Units - Ibs/million Ibs of aluminum product from rod
                             casting
 Acenaphthene
 Benzo(a)anthracene
*Benzo(a)pyrene
 Benzo(ghi)perylene
 Chrysene
 Dibenzo(a,h)anthracene
 Fluoranthene
 Pyrene
*Aluminum
*Antimony
 Arsenic
 Cadmium
 Chromium
 Copper
*Fluoride
 Lead
*Nickel
 Selenium
 Zinc

*Regulated Pollutant
    0.004
    0.008
    0.004
    0.004
    0.008
    0.004
    0.041
    0.028
    0.635
    0.201
    0.145
    0.021
    0.038
    0.133
    6.188
    0.029
    0.057
    0.085
    0.106
          0.002
          0.004
          0.002
          0.002
          0.004
          0.002
          0.019
          0.013
          0.282
          0.089
          0.064
          0.008
          0.016
          0.063
          2.746
          0.014
          0.038
          0.038
          0.044
                               806

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               PRIMARY ALUMINUM SUBCATEGORY   SECT - X


                      TABLE X-7 (Continued)

  BAT EFFLUENT LIMITATIONS FOR THE PRIMARY ALUMINUM SUBCATEGORY


        Stationary Casting or Shot Casting Contact Cooling
Pollutant or Pollutant Property
Maximum for
Any One Day
  Maximum for
Monthly Average
Metric Units - mg/kg of aluminum product from starionary casting
                         or shot casting
     English Units - Ibs/million Ibs of aluminum product from
                stationary casting or shot casting
 Acenaphthene
 Benzo(a)anthracene
*Benzo(a)pyrene
 Benzo(ghi)perylene
 Chrysene
 Dibenzo(a,h)anthracene
 Fluoranthene
 Pyrene
*Aluminum
*Antimony
 Arsenic
 Cadmium
 Chromium
 Copper
*Fluoride
 Lead
*Nickel
 Selenium
 Zinc

*Regulated Pollutant
    0.000
    0.000
    0.000
    0.000
    0.000
    0.000
    0.000
    0.000
    0.000
    0.000
    0.000
    0.000
    0.000
    0.000
    0.000
    0.000
    0.000
    0.000
    0.000
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          0.000
          0.000
          0.000
          0.000
          o.ooo
          0.000
          0.000
          0.000
          0.000
          0.000
          0.000
          0.000
          0.000
          0.000
          0.000
          0.000
          0.000
          0.000
                               807

-------
PRIMARY ALUMINUM SUBCATEGORY
SECT - X
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PRIMARY ALUMINUM SUBCATEGORY
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PRIMARY  ALUMINUM SUBCATEGORY
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PRIMARY ALUMINUM SUBCATEGORY   SECT - X
THIS PAGE INTENTIONALLY LEFT BLANK
               812

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              PRIMARY ALUMINUM SUBCATEGORY
                                     SECT - XI
                            SECTION XI

                 NEW SOURCE PERFORMANCE STANDARDS
The  basis  for  new source performance  standards  (NSPS)  under
Section  306  of  the  Act is  the  best  available  demonstrated
technology (BDT).   New plants have the opportunity to design the
best  and  most  efficient production  processes  and  wastewater
treatment  technologies,  without  facing  the  added  costs  and
restrictions  encountered  in  retrofitting  an  existing  plant.
Therefore/   Congress   directed   EPA  to  consider   the   best
demonstrated process changes,  in-plant controls, arid end-of-pipe
treatment  technologies  which  reduce pollution to  the  maximum
extent feasible.

This  section describes the control technology for  treatment  of
wastewater   from  new  sources,   and  presents  mass  discharge
limitations  of  regulated  pollutants  for  NSPS  based  on  the
described control technology.

TECHNICAL APPROACH TO BDT

All  of  the  treatment technology options applicable  to  a  new
source were previously considered for the BAT options.   For this
reason,  four options were considered for BDT that were identical
to  the BAT options discussed in Section X except for  Option  B.
Option  B eliminates three sources of wastewater through the  use
of  dry  air  pollution  control:   anode  paste  plant  wet  air
pollution  control,  anode bake plant wet air pollution  control,
and  potline  wet  air  pollution  control.   Degassing  wet  air
pollution  is also eliminated based on alternate in-line  fluxing
and filtering methods.  For all other waste streams, BDT Option B
is  identical to BAT Option B.   The treatment technologies  used
for the four BDT options are:

OPTION A

     o  Preliminary treatment with oil skimming (where required)
     o  Chemical precipitation and sedimentation
OPTION B

     o
     o

     o
     o
Preliminary treatment with oil skimming (where required)
Preliminary treatment of cathode reprocessing wastewater
with ferrous sulfate precipitation
Chemical precipitation and sedimentation
In-process flow reduction of casting contact cooling
water
Dry alumina scrubbing of gaseous emissions from anode
paste plants, anode bake plants, potlines, and potrooms
Alternate in-line fluxing and filtering techniques
                               813

-------
              PRIMARY ALUMINUM  SUBCATEGORY    SECT  - XI
 OPTION C
      o   Preliminary  treatment with oil skimming  (where  required)
      o   Preliminary  treatment of cathode  reprocessing wastewater
         with  ferrous sulfate precipitation
      o   Chemical precipitation and sedimentation
      o   In-process flow  reduction of casting contact cooling
         water
      o   Dry alumina  scrubbing of gaseous  emissions from anode
         paste plants, anode bake plants,  potlines, arid  pot rooms
      o   Alternate in-line fluxing and filtering techniques
      o   Multimedia filtration
OPTION E
     o
     o

     o
     o
     o
     o
     o
Preliminary treatment with oil skimming (where required)
Preliminary treatment of cathode reprocessing wastewater
with ferrous sulfate precipitation
Chemical precipitation and sedimentation
In-process flow reduction of casting contact cooling
water
Dry alumina scrubbing of gaseous emissions from anode
paste plants, anode bake plants, potlines, and potrooms
Alternate in-line fluxing and filtering techniques
Multimedia filtration
End-of-pipe treatment with activated carbon adsorption
Partial  or  complete  reuse  and recycle  of  wastewater  is  an
essential part of each option.   Reuse and recycle can precede or
follow  end-of-pipe  treatment.   A more detailed  discussion  of
these treatment options is presented in Section X.

BDT OPTION SELECTION

EPA proposed that the best available demonstrated technology  for
the  primary aluminum subcategory be based on BAT plus additional
flow reducbion.   Additional flow reduction was based on the  use
of  dry air pollution scrubbing on potlines,  anode bake  plants,
and  anode paste plants and elimination of potroom and  degassing
scrubber discharges.  Potroom scrubbing discharges are eliminated
by  design  of efficient potline scrubbing  (eliminating  potroom
scrubbing  completely) and the use of center worked prebake cells
and  side  worked Soderberg cells.   Zero  discharge  of  potline
scrubbing  is  also  demonstrated through the  reuse  of  casting
contact  cooling  water as  scrubber  liquor  makeup.   Degassing
scrubbers  are  eliminated through the use of  alternate  in-line
fluxing and filtering methods.

These  flow reductions are demonstrated at existing  plants,  but
were  not included in BAT because they might involve  substantial
retrofit costs at other existing plants.   However, new plants can
include  these  reductions  in  plant design  at  no  significant
additional cost.   Dry scrubbing also prevents the  contamination
of scrubbing discharges with toxic,organics.
                               814

-------
              PRIMARY ALUMINUM SUBCATEGORY   SECT - XI
Although  this technology is demonstrated,  information submitted
through comments and gathered by specific data requests indicates
that  two possible problems for new sources could be  created  by
the  proposed NSPS, one with respect to continued utilization  of
certain cell technologies, the other regarding ability to produce
certain high purity alloys.

Dry  potline scrubbing and elimination of potroom  scrubbing  for
new  sources  would effectively require center-worked prebake  or
horizontal stud Soderberg cell technology.   This is because  the
other  major  cell  technologies,  the  side-worked  prebake  and
vertical  Soderberg  cell,  must  use wet  scrubbers  to  control
fluoride  emissions due to hooding constraints.   EPA's NSPS  for
new  "green  field" primary aluminum sources are based  on  these
facilities   using  center-worked  prebake  and  horizontal  stud
Soderberg cells,  or achieving the effluent limitations that  are
associated   with  the  use  of  dry  scrubbing.    This  is   an
environmentally more acceptable process (particularly in terms of
net  effluent reductions) because fluoride emissions can be fully
contained  without the use of wet scrubbers while  capturing  and
returning the fluoride to the manufacturing process.   See Senate
Committee  on  Public Works,  A Legislative History of the  Clean
Water  Act,  93d  Cong.  1st Sess.,  Vol.  1 at 172  (new  source
performance standards are to reflect "levels of pollution control
which  are  available  through the  use  of  improved  production
processes)."

Ah  issue  arises,  however,  as to whether major  expansions  of
capacity at existing Soderberg plants are to be classified as new
sources or as major modifications subject to BAT.   Dry scrubbing
on  vertical  Soderberg potline or potroom emissions may  not  be
feasible, as a practical matter.  However, use of horizontal stud
Soderberg  technology with dry potline and not potroom  scrubbing
is demonstrated.  Therefore, construction of new sources or major
expansions  do  not receive a discharge allowance for potline  or
potroom scrubbing.

It  appears dry potline scrubbing may result in  product  quality
constraints  due to iron and silicon contamination when  recycled
alumina  from  scrubbers  is  used  as  potline  feed.    Industry
personnel report high purity alloys can be manufactured if only a
small  proportion  of  the plant's capacity is dedicated  to  the
manufacture  of  these alloys.    Thus,  it  appears  new  sources
producing   high   purity  alloys  would  be  at  a   competitive
disadvantage  if  they  must  install  dry  scrubbing  technology
because  of a requirement to use more virgin alumina per  ton  of
product.

The  Agency believes this problem to be hypothetical and unlikely
to  occur  in actuality.   Plants with dry  scrubbing  can  avoid
contamination  of these alloys  by segregating production of metal
produced  from  virgin  ore  from  metal  produced  from  alumina
recycled  from  dry scrubbers.    Although this may allow  only  a
relatively small (10 to 20)  percentage of a plant's production to
be dedicated to certain high purity alloys, EPA is unaware of any
                               815

-------
              PRIMARY ALUMINUM SUBCATEGORY   SECT - XI


plant  that devotes large percentages of its production  capacity
to these specific alloys.  Thus, all existing plants that produce
these  high  purity alloys and have dry scrubbers  appear  to  be
operating without competitive constraint.  Therefore, new sources
will  not suffer adverse competitive impact as a result of a  dry
scrubbing  requirement.   If a prospective new source is able  to
demonstrate  that (1) it will dedicate too much capacity to _high
purity alloys to utilize all of its recyclable alumina; (2) it is
unable to market its excess recyclable alumina; and (3) the costs
of  purchasing excess virgin ore and reprocessing alumina through
the Bayer process are so high as to pose a barrier to entry,  the
Agency will entertain rulemaking application to amend NSPS. Since
no demonstration has been made,  and the possibility appears very
remote, this proposed NSPS is not altered.

The  promulgated NSPS will eliminate discharge of toxic  organics
and   metals  associated  with  potline  and   potroom   scrubber
discharge,  but will not require any significantly different cost
of  compliance  for new or existing  sources.   The  incompatible
alloys with dry scrubbing are listed below:
     1.
     2.
     3.
     4.
     5.
1080
1085
1180
1188
2124
 6.
 7.
 8.
 9.
10.
5252
5657
7029
A356
A357
Alternate   in-line   fluxing  and  filtering   is   demonstrated
throughout  the subcategory.  However,  industry  representatives
claim  alternate in-line fluxing and filtering is not capable  of
manufacturing  all  alloys, and therefore, a  degassing  scrubber
allowance  is necessary so that furnace fluxing can be  used  for
new  sources.   Each  facility known  to  use  alternate  in-line
methods  was  contacted to determine if any of these  alloys  are
currently  manufactured  or capable of  being  manufactured  with
alternate  in-line fluxing.  Table XI-1 (page 818)  presents  the
results  of this survey.  As shown in the table,  manufacture  of
these  alloys  with  alternate  in-line  fluxing  techniques   is
possible.  Therefore, NSPS is based on alternate in-line  fluxing
and  filtering,  which  eliminates the  need  for  wet  degassing
scrubbers.

REGULATED POLLUTANT PARAMETERS

The Agency has no reason to believe that the pollutants that will
be  found  in  treatable concentrations in processes  within  new
sources  will  be  any  different  than  with  existing  sources.
Accordingly,  pollutants  and pollutant parameters  selected  for
limitation  under  NSPS,  in  accordance with  the  rationale  of
Sections VI and X,  are identical to those selected for BAT.  The
conventional pollutant parameters TSS, oil and grease, and pH are
also selected for limitation.
                                816

-------
              PRIMARY ALUMINUM SUBCATEGORY
SECT - XI
NEW SOURCE PERFORMANCE STANDARDS

The NSPS discharge flows for anode paste plant, anode bake plant,
potline air scrubbing,  and potroom air scrubbing will be zero as
a result of the use of dry air pollution controls.  Degassing wet
air  pollution  control is eliminated through  alternate  in-line
fluxing and filtering techniques.  The remaining stream discharge
flows are the same for all options and are presented in Table XI-
2 (page 819).  The mass of pollutant allowed to be discharged per
mass  of  product is calculated by  multiplying  the  appropriate
effluent  concentration  (Table VIII-21, Vol-l,page 248)  by.  the
production  normalized  wastewater discharge flows  (1/kkg).  New
source performance standards for the primary aluminum subcategory
waste streams are shown in Table XI-3 (page 821).

EPA  amended  the  pH standard for new sources for  direct  chill
casting  contact  cooling  water to a pH range  of  6.0  to  10.0
standard  units provided this stream is not commingled with other
process  wastewaters.   If direct chill casting  contact  cooling
water  is  •commingled  with other process  waters,  it  is  still
subject to a pH range of 7.0 to 10.0 at all times.
                                817

-------
              PRIMARY ALUMINUM SUBCATEGORY
                                     SECT -  XI
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-------
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-------
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-------
              PRIMARY ALUMINUM SUBCATEGORY   SECT - XI


                           TABLE XI-3

            NSPS FOR THE PRIMARY ALUMINUM SUBCATEGORY


     Anode and Cathode Paste Plant Wet Air Pollution Control
Pollutant or Pollutant Property
        Maximum for
        Any One Day
  Maximum for
Monthly Average
             Metric Units - mg/kg of paste produced
        English Units - Ibs/million Ibs of paste produced
 Acenaphthene
 Benzo(a)anthracene
*Benzo(a)pyrene
 Benzo(ghi)perylene
 Chrysene
 Dibenzo(a,h)anthracene
 Fluoranthene
 Phenanthrene
 Pyrene
*Aluminum
*Antimony
 Arsenic
 Cadmium
 Chromium
 Copper
*Fluoride
 Lead
*Nickel
 Selenium
 Zinc
*Oil & Grease
*TSS
*pH

*Regulated Pollutant
            0.000                0.000,
            0.000                0.000
            0.000                0.000
            0.000                0.000
            0.000                0.000
            0.000                0.000
            0.000                0.000
            0.000                0.000
            0.000                0.000
            0.000                0.000
            0.000                0.000
            0.000                0.000
            0.000                0.000
            0.000                0.000
            0.000                0.000
            0.000                0.000
            0.000                0.000
            0.000                0.000
            0.000                0.000
            0.000                0.000
            0.000                0.000
            0.000                0.000
Within the range of 7.0 to 10.0
       at all times
                               821

-------
               PRIMARY ALUMINUM  SUBCATEGORY    SECT - XI


                     TABLE Xl-3 (Continued)

            NSPS FOR THE PRIMARY ALUMINUM SUBCATEGORY


          Anode Contact Cooling and Briquette Quenching
Pollutant or Pollutant Property
        Maximum for
        Any One Day
  Maximum for
Monthly Average
               Metric Units - mg/kg of anodes cast
          English Units - Ibs/million Ibs of anodes cast
 Acenaphthene
 Benzo(a)anthracene
*Benzo(a)pyrene
 Benzo(ghi)perylene
 Chrysene
 Dibenzo(a, h)anthracene
 Pluoranthene
 Phenanthrene
 Pyrene
*Aluminum
*Antimony
 Arsenic
 Cadmium
 Chromium
 Copper
*Pluoride
 Lead
*Nickel
 Selenium
 Zinc
*Oil & Grease
*TSS
*pH

*Regulated Pollutant
            0.007                0.003
            0.016                0.007
            0.007                0.003
            0.007                0.003
            0.016                0.007
            0.007                0.003
            0.082                0.038
            0.007                0.003
            0.056                0.026
            1.277                0.566
            0.403                0.180
            0.291       '         0.130
            0.042                0.017
            0.077                0.031
            0.268                0.127
           12.440                5.518
            0.059                0.027
            0.115                0.077
            0.171                0.077
            0.213                0.088
            2.090                2.090
            3.135                2.508
Within the range of 7.0 to 10.0
       at all times
                               822

-------
              PRIMARY ALUMINUM SUBCATEGORY   SECT - XI


                     TABLE Xl-3 (Continued)

            NSPS FOR THE PRIMARY ALUMINUM SUBCATEGORY


          Anode Bake Plant Wet Air Pollution Control
Pollutant or Pollutant Property
        Maximum for
        Any One Day
  Maximum for
Monthly Average
             Metric Units - mg/kg of anodes baked
       English Units - Ibs/million Ibs of anodes baked
 Acenaphthene
 Benzo(a)anthracene
*Benzo(a)pyrene
 Benzo(ghi)perylene
 Chrysene
 Dibenzo(afh)anthracene
 Fluoranthene
 Pyrene
*Aluminum
*Antimony
 Arsenic
 Cadmium
 Chromium
 Copper
*Fluoride
 Lead
*Nickel
 Selenium
 Zinc
*Oil & Grease
*TSS
*pH

*Regulated Pollutant
            0.000                0.000
            0.000                0.000
            0.000                0.000
            0.000                0.000
            0.000            '    0.000
            0.000                0.000
            0.000                0.000
            0.000                0.000
            0.000                0.000
            0.000                0.000
            0.000                0.000
            0.000                0.000
            0.000                0.000
            0.000                0.000
            0.000                0.000
            0.000                0.000
            0.000                0.000
            0.000                0.000
            0.000                0.000
            0.000                0.000
            0.000                0.000
Within the range of 7.0 to 10.0
       at all times
                               823

-------
              PRIMARY ALUMINUM SUBCATEGORY
          SECT - XI
                     TABLE Xl-3 (Continued)

            NSPS FOR THE PRIMARY ALUMINUM SUBCATEGORY
       Cathode Reprocessing (Operated With Dry Potline
      Scrubbing and Not Commingled With Other Process or
                      Nonprocess Waters)
Pollutant or Pollutant Property
Maximum for
Any One Day
                         Maximum for
                       Monthly Average
          Metric Units - mg/kg of cryolite recovered
    English Units - Ibs/million Ibs of cryolite recovered
 Acenaphthene
 Benzo(a)anthracene
*Benzo(a)pyrene
 Benzo(ghi)perylene
 Chrysene
 Dibenzo(a,h)anthracene
 Fluoranthene
 Pyrene
*Aluminum
*Antimony
 Arsenic
 Cadmium
 Chromium
 Copper
*Cyanide
*Fluoride
 Lead
*Nickel
 Selenium
 Zinc
*Oil & Grease
*TSS
*pH

*Regulated Pollutant
    1.180
    2.715
      ,180
      ,180
    2.715
    1.
            1,
            1,
              ,180
           13.690
            9.326
          273.200
          420.400
           48.690
            7.006
           12.960
           44.840
          157.600
       29,430.000
            9.808
           80.570
           28.720
           35.730
          350.300
         2172.000
Within the range of 7
       at all times
            0.546
            1.257
            0.546
            0.546
            1.257
            0.546
            6.339
            4.317
          122.600
          189.200
           21.720
            2.802
            5.254
           21.370
           70.060
        3,310.000
            4.554
           35.030
           12.960
           14.710
          350.300
          945.800
, 0  to  10.0
                               824

-------
              PRIMARY ALUMINUM SUBCATEGORY   SECT - XI


                     TABLE XI-3 (Continued)

            NSPS FOR THE PRIMARY ALUMINUM SUBCATEGORY
         Cathode Reprocessing (Operated With Dry Potline
          Scrubbing and Commingled With Other Process or
                        Nonprocess Waters)
Pollutant or Pollutant Property
        Maximum for
        Any One Day
     Maximum for
   Monthly Average
            Metric Units - mg/kg of cryolite recovered
      English Units - Ibs/million Ibs of cryolite recovered
 Acenaphthene
 Benzo(a)anthracene
*Benzo(a)pyrene
 Benzo(ghi)perylene
 Chrysene
 Dibenzo(a,h)anthracene
 Fluoranthene
 Pyrene
*Aluminum
*Antimony
 Arsenic
 Cadmium
 Chromium
 Copper
*Cyanide
*Fluoride
 Lead
*Nickel
 Selenium
 Zinc
*Oil & Grease
*TSS
*pH

*Regulated Pollutant
            1.180
            2.715
            1.181
            1.180
            2.715
            1.180
           13.690
            9.326
          214.000
           67.600
           48.690
            7.006
           12.960
           44.840
          157.600
         2084.000
            9.808
           19.270
           28.720
           35.730
          350.300
         2172.000
Within the range of
       at all times
             0.546
             1.257
             0.547
             0.546
             1.257
             0.546
             6.339
             4.317
            94.930
            30.120
            21.720
             2.802
             5.254
            21.370
            70.060
           924.800
             4.554
            12.960
            12.960
            14.710
           350.300
           945.800
7.0 to 10.0
                               825

-------
               PRIMARY ALUMINUM  SUBCATEGORY   SECT - XI


                     TABLE Xl-3  (Continued)

            NSPS FOR THE PRIMARY ALUMINUM SUBCATEGORY


                Potline Wet Air Pollution Control
Pollutant or Pollutant Property
        Maximum for
        Any One Day
     Maximum for
   Monthly Average
   Metric Units - mg/kg of aluminum produced from electrolytic
                            reduction
    English Units - Ibs/million Ibs of aluminum produced from
                      electrolytic reduction
 Acenaphthene
 Benzo(a)anthracene
*Benzo(a)pyrene
 Benzo(ghi)perylene
 Chrysene
 Dibenzo(a,h)anthracene
 Pluoranthene
 Pyrene
*Aluminum
*Antimony
 Arsenic
 Cadmium
 Chromium
 Copper
*Pluoride
 Lead
*Nickel
 Selenium
 Zinc
*Oil & Grease
*TSS
*pH

*Regulated Pollutant
            0.000
            0.000
            0.000
            0.000
            0.000
            0.000
            0.000
            0.000
            0.000
            0.000
            0.000
            0.000
            0.000
            0.000
            0.000
            0.000
            0.000
            0.000
            0.000
            0.000
            0.000
Within the range of
       at all times
              .000
              .000
              .000
              .000
              .000
              .000
              .000
              .000
              .000
              .000
              .000
              .000
              .000
              .000
              .000
              .000
              .000
              .000
              .000
              .000
              .000
7.0 to 10.0
                               826

-------
              PRIMARY ALUMINUM SUBCATEGORY   SECT - XI


                     TABLE Xl-3 (Continued)

            NSPS FOR THE PRIMARY ALUMINUM SUBCATEGORY


                Potroom Wet Air Pollution Control
Pollutant or Pollutant Property
        Maximum for
        Any One Day
  Maximum for
Monthly Average
   Metric Units - mg/kg of aluminum produced from electrolytic
                            reduction
    English Units - Ibs/million Ibs of aluminum produced from
                      electrolytic reduction
 Acenaphthene
 Benzo(a)anthracene
*Benzo(a)pyrene
 Benzo(ghi)perylene
 Chrysene
 Dibenzo(a,h)anthracene
 Fluoranthene
 Pyrene
*Aluminum
*Antimony
 Arsenic
 Cadmium
 Chromium
 Copper
*Fluoride
 Lead
*Nickel
 Selenium
 Zinc
*Oil & Grease
*TSS
*pH

*Regulated Pollutant
            0.000
            0.000
            0.000
            0.000
            0.000
            0.000
            0.000
            0.000
            0.000
            0.000
            0.000
            0.000
            0.000
            0.000
            0.000
            0.000
            0.000
            0.000
            0.000
            0.000
            0.000
Within the range of 7.0
       at all times
          0.000
          0.000
          0.000
          0.000
          0.000
          0.000
          0.000
          0.000
          0.000
          0.000
          0.000
          0.000
          0.000
          0.000
          0.000
          0.000
          0.000
          0.000
          0.000
          0.000
          0.000
  to  10.0
                                827

-------
               PRIMARY ALUMINUM SUBCATEGORY
                   SECT  -  XI
                      TABLE  Xl-3  (Continued)

            NSPS  FOR  THE  PRIMARY ALUMINUM  SUBCATEGORY


        Potline SO2 Emissions Wet Air Pollution Control
Pollutant or Pollutant Property
        Maximum for
        Any One Day
   Maximum for
 Monthly Average
   Metric Units - mg/kg of aluminum produced from electrolytic
                            reduction
    English Units - Ibs/million Ibs of aluminum produced from
                      electrolytic reduction
 Acenaphthene
 Benzo(a)anthracene
*Benzo{a)pyrene
 Benzo(ghi)perylene
 Chrysene
 Dibenzo(a,h)anthracene
 Pluoranthene
 Pyrene
*Aluminum
*Antimony
 Arsenic
 Cadmium
 Chromium
 Copper
*Pluoride
 Lead
*Nickel
 Selenium
 Zinc
*Oil -& Grease
*TSS
*pH

*Regulated Pollutant
            0.045
            0.104
            0.045
            0.045
            0.104
            0.045
            0.524
            0.357
            8.194
            2.588
            1.864
            0.258
            0.496
            1.716
           79.790
            0.375
            0.738
            1.100
            1.368
           13*410
           20.120
Within the range of 7,
       at all times
           0.021
           0.048
           0.021
           0.021
           0.048
           0.021
           0.243
           0.165
           3.634
           1.153
           0.831
           0.107
           0.201
           0.818
          35.400
           0.174
           0.496
           0.496
           0.563
          13.410
          16.090
0 to 10.0
                               828

-------
              PRIMARY ALUMINUM SUBCATEGORY
                  SECT - XI
                     TABLE Xl-3 (Continued)

            NSPS FOR THE PRIMARY ALUMINUM SUBCATEGORY


               Degassing Wet Air Pollution Control
Pollutant or Pollutant Property
        Maximum for
        Any One Day
     Maximum for
   Monthly Average
   Metric Units - mg/kg of aluminum produced from electrolytic
                            reduction
    English Units - Ibs/million Ibs of aluminum produced from
                           electrolytic reduction
 Acenaphthene
 Benzo{a)anthracene
*Benzo(a)pyrene
 Benzo(ghi)perylene
 Chrysene
 Dibenzo(afh)anthracene
 Fluoranthene
 Pyrene
*Aluminum
*Antimony
 Arsenic
 Cadmium
 Chromium
 Copper
*Fluoride
 Lead
*Nickel
 Selenium
 Zinc
*Oil & Grease
*TSS
*pH

*Regulated Pollutant
            0.000
            0.000
            0.000
            0.000
            0.000
            0.000
            0.000
            0.000
            0.000
            0.000
            0.000
            0.000
            0.000
            0.000
            0.000
            0.000
            0.000
            0.000
            0.000
            0.000
            0.000
Within the range of
       at all times
              .000
              .000
              .000
              .000
              .000
              .000
              .000
              .000
              .000
              .000
              .000
              .000
              .000
              .000
              .000
              .000
              .000
              .000
              .000
              .000
              .000
7.0 to 10.0
                               829

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              PRIMARY ALUMINUM  SUBCATEGORY   SECT - XI


                     TABLE Xl-3  (Continued)

            NSPS FOR THE PRIMARY ALUMINUM SUBCATEGORY


                    Pot Repair and Pot Soaking
Pollutant or Pollutant Property
        Maximum for
        Any One Day
   Maximum for
 Monthly Average
   Metric Units - mg/kg of aluminum produced from electrolytic
                             refining
    English Units - Ibs/million Ibs of aluminum produced from
                      electrolytic reduction
 Acenaphthene
 Benzo(a)anthracene
*Benzo(a)pyrene
 Benzo(ghi)perylene
 Chrysene
 Dibenzo(a,h)anthracene
 Fluoranthene
 Pyrene
*Aluminum
*Antimony
 Arsenic
 Cadmium
 Chromium
 Copper
*Fluoride
 Lead
*Nickel
 Selenium
 Zinc
*Oil & Grease
*TSS
*pH

*Regulated Pollutant
            0.000
            0.000
            0.000
            0.000
            0.000
            0.000
            0.000
            0.000
            0.000
            0.000
            0.000
            0.000
            0.000
            0.000
            0.000
            0.000
            0.000
            0.000
            0.000
            0.000
            0.000
Within the range of 7
       at all times
           0.000
           0.000
           0.000
           0.000
           0.000
           0.000
           0.000
           0.000
           0.000
           0.000
           0.000
           0.000
           0.000
           0.000
           0.000
           0.000
           0.000
           0.000
           0.000
           0.000
           0.000
0 to 10.0
                               830

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              PRIMARY  ALUMINUM SUBCATEGORY    SECT  -  XI


                    TABLE Xl-3 (Continued)

            NSPS FOR THE PRIMARY ALUMINUM SUBCATEGORY
              Direct Chill Casting Contact Cooling
Pollutant or Pollutant Property
        Maximum for
        Any  One Day
                                                    Maximum for
                                                  Monthly Average
   Metric Units - mg/kg of aluminum product from direct chill
                             casting
     English Units - Ibs/million Ibs of aluminum product from
                         direct chill casting
 Acenaphthene
 Benzo(a)anthracene
*Benzo(a)pyrene
 Benzo(ghi)perylene
 Chrysene
 Dibenzo(a,h)anthracene
 Fluoranthene
 Pyrene
*Aluminum
*Antimony
 Arsenic
 Cadmium
 Chromium
 Copper
*Fluoride
 Lead
*Nickel
 Selenium  '
 Zinc
*Oil & Grease
*TSS
*pH

*Regulated Pollutant
            0.045
            0.103
            0.045
            0.045
            0.103
            0.045
            0.520
            0.354
            8.120
            2.565
            1.847
            0.266
            0.492
            1.701
           79.080
            0.372
            0.731
            1.090
            1.356
           13.290
           19.940
Within the range of 7.0
       at all times
                                                            0.021
                                                            0.048
                                                            0.021
                                                            0.021
                                                            0.048
                                                            0.021
                                                            0.240
                                                            0.164
                                                            3.602
                                                            1.143
                                                            0.824
                                                            0.106
                                                            0.199
                                                            0.811
                                                           35.090
                                                            0.173
                                                            0.492
                                                            0.492
                                                            0.558
                                                           13.290
                                                           15.950
                                                   to 10.0
                                831

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               PRIMARY ALUMINUM SUBCATEGORY   SECT - XI


                      TABLE Xl-3 (Continued)

             NSPS FOR THE PRIMARY ALUMINUM SUBCATEGORY


               Continuous Rod Casting Contact  Cooling
 Pollutant  or  Pollutant  Property
         Maximum for
         Any  One Day
   Maximum  for
 Monthly Average
    Metric  Units  -  mg/kg  of  aluminum product  from  rod casting
     English  Units  -  Ibs/million  Ibs of  aluminum product from
                           rod  casting
 Acenaphthene
 Benzo(a)anthracene
*Benzo(a)pyrene
 Benzo(ghi)perylene
 Chrysene
 Dibenzo(a,h)anthracene
 Fluoranthene
 Pyrene
*Aluminum
*Antimony
 Arsenic
 Cadmium
 Chromium
 Copper
*Fluoride
 Lead
*Nickel
 Selenium
 Zinc
*Oil & Grease
*TSS
*pH

*Regulated Pollutant
             0.004
             0.008
             0.004
             0.004
             0.008
             0.004
             0.041
             0.028
             0.635
             0.201
             0.145
             0.021
             0.038
             0.133
             6.188
             0.029
             0.057
             0.085
             0.106
             1.040
             1.560
Within the range of 7
       at all times
           0.002
           0.004
           0.002
           0.002
           0.004
           0.002
           0.019
           0.013
           0.282
           0.089
           0.064
           0.008
           0.016
           0.063
           2.746
           0.014
           0.038
           0.038
           0.044
           1.040
           1.248
0 to 10.0
                               832

-------
              PRIMARY ALUMINUM SUBCATEGORY   SECT -.XI


                        TABLE Xl-3 (Continued)

            NSPS FOR THE PRIMARY ALUMINUM SUBCATEGORY


     Stationary Casting or Shot Casting Contact Cooling
Pollutant or Pollutant Property
        Maximum for
        Any One Day
   Maximum for
 Monthly Average
 Metric Units - mg/kg of aluminum product from stationary casting
                         or shot casting
      English Units - Ibs/million Ibs of aluminum product from
                stationary casting or shot casting
 Acenaphthene
 Benzo(a)anthracene
*Benzo (a) py'r ene
 Benzo(ghi)perylene
 Chrysene
 Dibenzo(a,h)anthracene
 Fluoranthene
 Pyrene
*Aluminum
*Antimony
 Arsenic
 Cadmium
 Chromium
 Copper
*Fluoride
 Lead
*Nickel
 Selenium
 Zinc
*Oil & Grease
*TSS
*pH

*Regulated Pollutant
            0.000
            0.000
            0.000
            0.000
            0.000
            0.000
            0.000
            0.000
            0.000
            0.000
            0.000
            0.000
            0.000
            0.000
            0.000
            0.000
            0.000
            0.000
            0.000
            0.000
            0.000
Within the range of 7
       at all times
           0.000
           0.000
           0.000
           0.000
           0.000
           0.000
           0.000
           0.000
           0.000
           0.000
           0.000
           0.000
           0.000
           0.000
           0.000
           0.000
           0.000
           0.000
           0.000
           0.000
           0.000
0 to 10.0
                               833

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PRIMARY ALUMINUM SUBCATEGORY   SECT - XI
 THIS PAGE INTENTIONALLY LEFT BLANK
                834

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              PRIMARY ALUMINUM SUBCATEGORY   SECT - XII




                           SECTION XII

                      PRETREATMENT STANDARDS
Section 307(b) of the Act requires EPA to promulgate pretreatment
standards  for  existing sources (PSES),  which must be  achieved
within three years of promulgation.  PSES are designed to prevent
the discharge of pollutants which pass through,  interfere  with,
or  are  otherwise  incompatible with the operation  of  publicly
owned  treatment  works  (POTW).   The Clean Water  Act  of  1977
requires pretreatment for pollutants,  such as heavy metals, that
limit POTW sludge management alternatives.  Section 307(c) of the
Act  requires  EPA to promulgate pretreatment standards  for  new
sources  (PSNS) at the same time that it promulgates  NSPS.   New
indirect   discharge  facilities,   like  new  direct   discharge
facilities,   have  the  opportunity  to  incorporate  the   best
available  demonstrated technologies,  including process changes,
in-plant controls, and end-of-pipe treatment technologies, and to
use  plant  site selection to ensure  adequate  treatment  system
installation.  Pretreatment standards are to be technology-based,
analogous  to the best available technology for removal of  toxic
pollutants.

This section describes the control and treatment technologies for
pretreatment  of  process  wastewaters from new  sources  in  the
primary  aluminum  subcategory.   Mass discharge  limitations  of
regulated pollutants are presented based on the described control
technology.

TECHNICAL APPROACH TO PRETREATMENT

Before  proposing  and promulgating pretreatment  standards,  the
Agency examines whether the pollutants discharged by the industry
pass through the POTW or interfere with the POTW operation or its
chosen  sludge  disposal  practices.    In  determining   whether
pollutants pass through a well-operated POTW, achieving secondary
treatment,  the  Agency  compares the percentage of  a  pollutant
removed  by POTW with the percentage removed by direct discharger
applying the best available technology economically achievable. A
pollutant  is  deemed to pass through the POTW when  the  average
percentage  removed  nationwide by  well-operated  POTW,  meeting
secondary  treatment requirements,  is less than  the  percentage
removed   by  direct  dischargers  complying  with  BAT  effluent
limitations guidelines for that pollutant.  (See generally, 46 FR
at 9415-16 (January 28, 1981).)

This   definition  of  pass  through  satisfies   two   competing
objectives  set  by Congress:    (1) that  standards  for  indirect
dischargers  be  equivalent to standards  for direct  dischargers,
while  at the same time,   (2) that the treatment  capability  and
performance  of the POTW be recognized and taken into account  in
                                835

-------
               PRIMARY ALUMINUM  SUBCATEGORY
                                      SECT - XII
 regulating  the  discharge of pollutants from  indirect dischargers.
 The  Agency  compares percentage  removal rather than the mass  or
 concentration  of pollutants discharged because the latter  would
 not  take into  account the mass of pollutants discharged  to  the
 POTW   from  non-industrial  sources  nor  the  dilution  of  the
 pollutants   in  the POTW effluent  to lower concentrations  due  to
 the addition of large amounts of  non-industrial wastewater.

 PRETREATMENT STANDARDS FOR EXISTING SOURCES

 There  are  no indirect discharging primary aluminum plants in the
 United  States.   Consequently,   the  Agency has elected  to  not
 promulgate  pretreatment standards for existing sources.

 PRETREATMENT STANDARDS FOR NEW SOURCES

 Options  for pretreatment of wastewaters are based on  increasing
 the effectiveness of end-of-pipe  treatment technologies.  All in-
 plant changes and applicable end-of-pipe treatment processes have
 been discussed  previously in Sections X and XI.   The options for
 PSNS,  therefore,  are the same as the NSPS options discussed  in
 Section XI.   Although oil and grease is a conventional pollutant
 compatible   with  treatment  provided by POTW,  oil  skimming  is
 needed  for   the  PSNS  treatment  technology  to  ensure  proper
 removal.    Oil  and grease interferes with the chemical  addition
 and mixing  required for chemical precipitation treatment

A description of each option is presented in Section X,  while  a
more detailed discussion, including pollutants controlled by each
 treatment  process  and  achievable treatment  concentrations  is
presented in  Section VII of Vol-1.

Treatment technology options for the PSNS are:

OPTION A

     o  Preliminary treatment with oil skimming (where required)
     o  Chemical precipitation and sedimentation
OPTION B

     o
     o

     o
     o
Preliminary treatment with oil skimming (where required)
Preliminary treatment of cathode reprocessing wastewater
with ferrous sulfate precipitation
Chemical precipitation and sedimentation
In-process flow reduction of casting contact cooling
water
     o  Dry alumina scrubbing of gaseous emissions from anode
        paste plants, anode bake plants, potlines, and potrooms
     o  Alternate in-line fluxing and filtering
                               836

-------
              PRIMARY ALUMINUM SUBCATEGORY   SECT - XII
OPTION C
     o
     O

     o
     O
     o
     o
Preliminary treatment with oil skimming (where required)
Preliminary treatment of cathode reprocessing wastewater
with ferrous sulfate precipitation
Chemical precipitation and sedimentation
In-process flow reduction of casting contact cooling
water                                 .
Dry alumina scrubbing of gaseous emissions from anode
paste plants, anode bake plants, potlines, and potrooms
Alternate in-line fluxing and filtering
Multimedia filtration
OPTION E

     o  Preliminary treatment with oil skimming  (where required)
     o  Preliminary treatment of cathode reprocessing wastewater
        with ferrous sulfate precipitation
     o  Chemical precipitation and sedimentation
     o  In-process flow reduction of casting contact cooling
        water
     o  Dry alumina scrubbing of gaseous emissions from anode
        paste plants, anode bake plants, potlines, and potrooms
     o  Alternate in-line fluxing and filtering
     o  Multimedia filtration
     o  End-of-pipe treatment with activated carbon adsorption


PSNS OPTION SELECTION

The  technology basis for promulgated 3PSNS  is  identical   to  NSPS
 (Option   C).    The  treatment   scheme  consists of  preliminary
treatment with   ferrous sulfate precipitation and  oil   skimming
 (where required),  followed by lime precipitation, sedimentation,
in-process flow reduction, dry alumina scrubbing, and filtration.
EPA  knows  of  no  demonstrated technology that  provides  more
efficient pollutant removal than NSPS and BAT  technology.

New  plants have  the opportunity to design  and use the  best  and
most   efficient   nonferrous  metals manufacturing  processes  and
wastewater treatment technologies without facing the added costs
and   restrictions encountered  in retrofitting  an existing plant.
The   additional   flow  reduction  proposed  for new sources   can   be
achieved  by  the  use of  dry air  pollution scrubbing.    The Agency
believes  that  the  installation  of  dry scrubbing instead   of  wet
 scrubbing  in  new   facilities  reduces the   cost of  end-of-pipe
 treatment  by    reducing   the   overall   volume   of    wastewater
 discharged.

 REGULATED POLLUTANT  PARAMETERS

 Pollutants   and  pollutant  parameters  selected for  limitation_  in
 accordance  with the  rationale  of Sections VI and X,  are identical
 to those  selected for  limitation for  BAT  with  one exception.   EPA
 is promulgating PSNS  for  benzo(a)pyrene,   cyanide,   nickel,   and
                                837

-------
              PRIMARY ALUMINUM  SUBCATEGORY   SECT - XII
 fluoride  to prevent pass-through.   Limitations for antimony have
 not  been established  because  it was shown that a  well-operated
 POTW   removes  60 percent and the Agency estimates the  model  BAT
 treatment technology will  remove 55 percent.   The  conventional
 pollutants   are   not  limited  under  PSNS  because  they   are
 effectively  controlled by POTW.   Aluminum  is  not  regulated
 because POTW often use  it as an aid to enhance settling.

 PRETREATMENT STANDARDS

 The  PSNS  discharge flows  are identical to  the  NSPS  discharge
 flows  for  all processes.   These discharge flows are listed  in
 Table  XII-1   (page 839).   The mass of pollutant allowed  to  be
 discharged  per mass of product is calculated by multiplying  the
 achievable  treatment concentration (mg/1) (Table VII-21,  Vol-1,
 page   248) by the normalized wastewater discharge  flow  (1/kkg).
 Pretreatment  standards for new sources, as determined  from  the
 above  procedure,  are  shown in Table XII-2 (page 841)  for  each
 waste  stream.

Mass-based  standards  are promulgated for the  primary  aluminum
 subcategory to ensure that  the standards are achieved by means of
pollutant removal rather than by dilution.  They are particularly
 important  since  the  standards are based upon  flow  reduction;
pollutant  limitations associated with flow reduction  cannot  be
measured by any other way but as a reduction of mass discharged.
                               838

-------
        PRIMARY ALUMINUM SUBCATEGORY
              SECT  - "XII
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-------
          PRIMARY ALUMINUM SUBCATEGORY
SECT - XII
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                               840

-------
              PRIMARY ALUMINUM SUBCATEGORY   SECT - XII


                           TABLE XII-2

            PSNS FOR THE PRIMARY ALUMINUM SUBCATEGORY


     Anode and Cathode Paste Plant Wet Air Pollution Control
Pollutant or Pollutant Property
Maximum for
Any One Day
  Maximum for
Monthly Average
             Metric Units - mg/kg of paste produced
        English Units - Ibs/million Ibs of paste produced
 Acenaphthene
 Benzo(a)anthracene
*Benzo(a)pyrene
 Benzo(ghi)perylene
 Chrysene
 Dibenzo(afh)anthracene
 Fluoranthene
 Pyrene
 Antimony
 Arsenic
 Cadmium
 Chromium
 Copper
*Fluoride
 Lead
*Nickel
 Selenium
 Zinc

*Regulated Pollutant
    0.000
    0.000
    0.000
    0.000
    0.000
    0.000
    0.000
    0.000
    0.000
    0.000
    0.000
    0.000
    0.000
    0.000
    0.000
    0.000
    0.000
    0.000
          0.000
          0.000
          0.000
          0.000
          0.000
          0.000
          0.000
          0.000
          0.000
          0.000
          0.000
          0.000
          0.000
          0.000
          0.000
          0.000
          0.000
          0.000
                                841

-------
              PRIMARY ALUMINUM SUBCATEGORY   SECT - XII


                     TABLE XII-2  (Continued)

            PSNS FOR THE PRIMARY ALUMINUM SUBCATEGORY


          Anode Contact Cooling and Briquette Quenching
Pollutant or Pollutant Property
Maximum for
Any One Day
  Maximum for
Monthly Average
               Metric Units - mg/kg of anodes cast
          English Units - Ibs/million Ibs of anodes cast
 Acenaphthene
 Benzo(a)anthracene
*Benzo(a)pyrene
 Benzo(ghi)perylene
 Chrysene
 Dibenzo(a,h)anthracene
 Fluoranthene
 Pyrene
 Antimony
 Arsenic
 Cadmium
 Chromium
 Copper
*Fluoride
 Lead
*Nickel
 Selenium
 Zinc

*Regulated Pollutant
    0.007
    0.016
    0.007
    0.007
    0.016
    0.007
    0.082
    0.056
    0.403
    0.291
    0.042
    0.077
    0.268
   12.440
    0.059
    0.115
    0.171
    0.213
          0.003
          0.007
          0.003
          0.003
          0.007
          0.003
          0.038
          0.026
          0.180
          0.130
          0.017
          0.031
          0.127
          5.518
          0.027
          0.077
          0.077
          0.088
                               842

-------
              PRIMARY ALUMINUM SUBCATEGORY   SECT - XII


                     TABLE XII-2 (Continued)

            PSNS FOR THE PRIMARY ALUMINUM SUBCATEGORY


            Anode Bake Plant Wet Air Pollution Control
Pollutant or Pollutant Property
Maximum for
Any One Day
  Maximum for
Monthly Average
              Metric Units - mg/kg of anodes baked
         English Units - Ibs/million Ibs of anodes baked
 Acenaphthene
 Benzo(a)anthracene
*Benzo(a)pyrene
 Benzo(ghi)perylene
 Chrysene
 Dibenzo(a,h)anthracene
 Fluoranthene
 Pyrene
 Antimony
 Arsenic
 Cadmium
 Chromium
 Copper
*Fluoride
 Lead
*Nickel
 Selenium
 Zinc

*Regulated Pollutant
    0.000
    0.000
    0.000
    0.000
    0.000
    0.000
    0.000
    0.000
    0.000
    0.000
    0.000
    0.000
    0.000
    0.000
    0.000
    0.000
    0.000
    0.000
          0.000
          0.000
          0.000
          0.000
          0.000
          0.000
          0.000
          0.000
          0.000
          0.000
          o.oop
          0.000
          0.000
          0.000
          0.000
          0.000
          0.000
          0.000
                                843

-------
              PRIMARY ALUMINUM SUBCATEGORY
          SECT - XII
                     TABLE XII-2 (Continued)

            PSNS FOR THE PRIMARY ALUMINUM SUBCATEGORY
         Cathode Reprocessing (Operated With Dry Potline
       Scrubbing and Not Commingled With Other Process or
                       Nonprocess Waters)
Pollutant or Pollutant Property
Maximum for
Any One Day
                Maximum for
              Monthly Average
            Metric Units - mg/kg of cryolite recovered
      English Units - Ibs/million Ibs of cryolite recovered
 Acenaphthene
 Benzo(a)anthracene
*Benzo(a)pyrene
 Benzo(ghi)perylene
 Chrysene
 Dibenzo(a,h)anthracene
 Pluoranthene
 Pyrene
 Antimony
 Arsenic
 Cadmium
 Chromium
 Copper
*Cyanide
*Pluoride
 Lead
*Nickel
 Selenium
 Zinc

*Regulated Pollutant
   1.180
   2.715
   1.181
   1.180
   2.715
   1.1BO
  13.690
   9.326
  67.600
  48.690
   7.006
  12.960
  44.840
 157.600
2084.000
   9.808
  19.270
  28.720
  35.730
                         0.546
                         1.257
                         0.547
                         0.546
                         1.257
                         0.546
                         6.339
                         4.317
                        30.120
                        21.720
                         2.802
                         5.254
                        21.370
                        70.060
                       924.700
                         4,554
                        12.960
                        12.960
                        14.710
                               844

-------
              PRIMARY ALUMINUM SUBCATEGORY   SECT - XII


                     TABLE XII-2 (Continued)

            PSNS FOR THE PRIMARY ALUMINUM SUBCATEGORY
         Cathode Reprocessing (Operated With Dry Potline
         Scrubbing and Commingled With Other Process or
                       Nonprocess Waters)
Pollutant or Pollutant Property
 Maximum for
 Any One Day
  Maximum for
Monthly Average
            Metric Units - mg/kg of cryolite recovered
      English Units - Ibs/million Ibs of cryolite recovered
 Acenaphthene
 Benzo(a)anthracene
*Benzo(a)py"rene
 Benzo(ghi)perylene
 Chrysene
 Dibenzo(a,h)anthracene
 Fluoranthene
 Pyrene
 Antimony
 Arsenic
 Cadmium
 Chromium
 Copper
*Cyanide
*Fluoride
 Lead
*Nickel
 Selenium
 Zinc

*Regulated Pollutant
     1.180
     2.715
     1.181
     1.180
     2.715
     1.180
    13.690
     9.326
    67.600
    48.690
     7.006
    12.960
    44.840
   157.600
29,430.000
     9.808
    80.570
    28.720
    35.730
          0.546
          1.257
          0.547
          0.546
          1.257
          0.546
          6.339
          4.317
         30.120
         21.720
          2.802
          5.254
         21.370
         70.060
      3,310.000
          4.554
         35.030
         12.960
         14.710
                               845

-------
               PRIMARY ALUMINUM  SUBCATEGORY   SECT - XII



                     Table XII-2  (Continued)

           PSNS FOR THE PRIMARY ALUMINUM SUBCATEGORY
                Potline Wet Air Pollution Control
Pollutant or Pollutant Property
Maximum for
Any One Day
  Maximum for
Monthly Average
   Metric Units - mg/kg of aluminum produced from electrolytic
                            reduction
    English Units - Ibs/million Ibs of aluminum produced from
                      electrolytic reduction
 Acenaphthene
 Benzo(a)anthracene
*Benzo(a)pyrene
 Benzo(ghi)perylene
 Chrysene
 Dibenzo(a,h)anthracene
 Fluoranthene
 Pyrene
 Antimony
 Arsenic
 Cadmium
 Chromium
 Copper
*Fluoride
 Lead
*Nickel
 Selenium
 Zinc

*Regulated Pollutant
    0.000
    0.000
    0.000
    0.000
    0.000
    0.000
    0.000
    0.000
    0.000
    0.000
    0.000
    0.000
    0.000
    0.000
    0.000
    0.000
    0.000
    0.000
          0.000
          0.000
          0.000
          0.000
          0.000
          0.000
          0.000
          0.000
          o.ooo
          0.000
          0.000
          0.000
          0.000
          0.000
          0.000
          0.000
          0.000
          0.000
                               846

-------
              PRIMARY ALUMINUM SUBGATEGORY   SECT - XII


                     TABLE XII-2 (Continued)

            PSNS FOR THE PRIMARY ALUMINUM SUBCATEGORY


                Potroom Wet Air Pollution Control
Pollutant or Pollutant Property
Maximum for
Any One Day
  Maximum for
Monthly Average
   Metric Units - mg/kg of aluminum produced from electrolytic
                            reduction
    English Units - Ibs/million Ibs of aluminum produced from
                      electrolytic reduction
 Acenaphthene
 Benzo(a)anthracene
*Benzo(a)pyrene
 Benzo(ghi)perylene
 Chrysene
 Dibenzo(a,h)anthracene
 Fluoranthene
 Pyrene
 Antimony
 Arsenic
 Cadmium
 Chromium
 Copper .
*Fluoride
 Lead
*Nickel
 Selenium
 Zinc

*Regulated Pollutant
    0.045
    0.104
    0.045
    0.045
    0.104
    0.045
    0.524
    6.357
    2.588
    1.864
    0.268
    0.496
    1.716
   79.790
    0.375
    0.738
    1.100
    1.368
          0.021
          0.048
          0.021
          0.021
          0.048
          0.021
          0.243
          0".165
          1.153
          0.831
          0.107
          0.201
          0.818
         35.400
          0.174
          0.496
          0.496
         • 0.563
                               847

-------
              PRIMARY ALUMINUM SUBCATEGORY   SECT - XII


                     TABLE XII-2 (Continued)

            PSNS FOR THE PRIMARY ALUMINUM SUBCATEGORY


        Potline SO? Emissions Wet Air Pollution Control
Pollutant or Pollutant Property
Maximum for
Any One Day
  Maximum for
Monthly Average
   Metric Units - mg/kg of aluminum produced from electrolytic
                            reduction
      English Units - Ibs/million Ibs of aluminum produced from
                      electrolytic reduction
 Acenaphthene
 Benzo(a)anthracene
*Benzo(a)pyrene
 Benzo(ghi)perylene
 Chrysene
 Dibenzo(a,h)anthracene
 Pluoranthene
 Pyrene
 Antimony
 Arsenic
 Cadmium
 Chromium
 Copper
*Fluoride
 Lead
*Nickel
 Selenium
 Zinc

*Regulated Pollutant
    0.000
    0.000
    0.000
    0.000
    0.000
    0.000
    0.000
    0.000
    0.000
    0.000
    0.000
    0.000
    0.000
    d.ooo
    0.000
    0.000
    0.000
    0.000
          0.000
          0.000
          0.000
          0.000
          0.000
          0.000
          0.000
          0.000
          0.000
          0.000
          0.000
          0.000
          0.000
          0.000
          0.000
          0.000
          0.000
          0.000
                               848

-------
              PRIMARY ALUMINUM SUBCATEGORY
          SECT - XII
                     Table X1I-2 (Continued)

            PSNS FOR THE PRIMARY ALUMINUM SUBCATEGORY


               Degassing Wet Air Pollution Control
Pollutant or Pollutant Property
Maximum for
Any One Day
  Maximum for
Monthly Average
   Metric Units - mg/kg of aluminum produced from electrolytic
                            reduction
    English Units - Ibs/million Ibs of aluminum produced from
                      electrolytic reduction
 Acenaphthene
 Benzo(a)anthracene
*Benzo(a)pyrene
 Benzo(ghi Jperylene
 Chrysene
 Dibenzo(a,h)anthracene
 Fluoranthene
 Pyrene
 Antimony
 Arsenic
 Cadmium
 Chromium
 Copper
*Fluoride
 Lead
*Nickel
 Selenium
 Zinc

*Regulated Pollutant
    0.000
    0.000
    0.000
    0.000
    0.000
    0.000
    0.000
    0.000
    0.000
    0.000
    0.000
    0.000
    0.000
    0.000
    0.000
    0.000
    0.000
    0.000
          0.000
          0.000
          0.000
          0.000
          0.000
          0.000
          0.000
          0.000
          0.000
          0.000
          0.000
          0.000
          0.000
          0.000
          0.000
          0.000
          0.000
          0.000
                               849

-------
              PRIMARY ALUMINUM SUBCATEGORY   SECT - XII


                     TABLE XII-2  (Continued)

            PSNS FOR THE PRIMARY ALUMINUM SUBCATEGORY


                    Pot Repair and Pot Soaking
Pollutant or Pollutant Property
Maximum for
Any One Day
  Maximum for
Monthly Average
   Metric Units - mg/kg of aluminum produced from electrolytic
                            reduction
    English Units - Ibs/million Ibs of aluminum produced from
                      electrolytic reduction
 Acenaphthene
 Benzo(a)anthracene
*Benzo(a)pyrene
 Benzo(ghi)perylene
 Chrysene
 Dibenzo(afh)anthracene
 Fluoranthene
 Pyrene
 Antimony
 Arsenic
 Cadmium
 Chromium
 Copper
*Fluoride
 Lead
*Nickel
 Selenium
 Zinc

*Regulated Pollutant
    0.000
    0.000
    0.000
    0.000
    0.000
    0.000
    0.000
    0.000
    0.000
    0.000
    0.000
    0.000
    0.000
    0.000
    0.000
    0.000
    0.000
    0.000
          0.000
          0.000
          0.000
          0.000
          0.000
          0.000
          0.000
          0.000
          0.000
          0.000
          0.000
          0.000
          0.000
          0.000
          0.000
          0.000
          0.000
          0.000
                               850

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              PRIMARY ALUMINUM SUBCATEGORY
          SECT - XII
                     TABLE XII-2 (Continued)

            PSNS FOR THE PRIMARY ALUMINUM SUBCATEGORY


              Direct Chill Casting Contact Cooling
Pollutant or Pollutant Property
Maximum for
Any One Day
  Maximum for
Monthly Average
   Metric Units - mg/kg of aluminum product from direct chill
                             casting
     English Units - Ibs/million Ibs of aluminum product from
                       direct chill casting
 Acenaphthene
 Benzo(a)anthracene
*Benzo(a)pyrene       :
 Benzo(ghi)perylene
 Chrysene
 Dibenzo(a,h)anthracene
 Fluoranthene
 Pyrene
 Antimony
 Arsenic
 Cadmium
 Chromium
 Copper
*Fluoride
 Lead
*Nickel
 Selenium
 Zinc

*Regulated Pollutant
    0.045
    0.103
    0.045
    0.045
    0.103
    0.045
    0.520
    0.354
    2.565
    1.847
    0.266
    0.492
    1.701
   79.080
    0.372
    0.731
    1.090
    1.356
          0.021
          0.048
          0.021
          0.021
          0.048
          0.021
          0.240
          0.164
          1.143
          0.824
          0.106
          0.199
          0.811
         35.090
          0.173
          0.492
          0.492
          0.558
                               851

-------
               PRIMARY ALUMINUM SUBCATEGORY   SECT  -  XII




                      Table  Xll-2  (Continued)

             PSNS  FOR THE  PRIMARY  ALUMINUM  SUBCATEGORY


               Continuous  Rod  Casting  Contact  Cooling
Pollutant or Pollutant Property
Maximum for
Any One Day
  Maximum for
Monthly Average
    Metric Units - mg/kg of aluminum product from rod casting
     English Units - Ibs/million Ibs of aluminum product from
                          rod casting

 Acenaphthene                          0.004                0.002
 Benzo(a)anthracene                    0.008                0.004
*Benzo(a)pyrene                        0.004                0.002
 Benzo(ghi)perylene                    0.004                0.002
 Chrysene                              0.008                0.004
 Dibenzo(a,h)anthracene                0.004                0.002
 Fluoranthene                          0.041                0.019
 Pyrene                                0.028                0.013
 Antimony                              0.201                0.089
 Arsenic                               0.145                0.064
 Cadmium                               0.021                0.008
 Chromium                              0.038                0.016
 Copper                                0.133                0.063
*Fluoride                              6.188                2.746
 Lead                                  0.029                0.014
*Nickel                                0.057                0.038
 Selenium                              0.085                0.038
 Zinc                                  0.106                0.044

*Regulated Pollutant
                               852

-------
              PRIMARY ALUMINUM SUBCATEGORY
          SECT - XII
                     TABLE XI1-2 (Continued)

            PSNS FOR THE PRIMARY ALUMINUM SUBCATEGORY


        Stationary Casting or Shot Casting Contact Cooling
Pollutant or Pollutant Property
Maximum for
Any One Day
  Maximum for
Monthly Average
Metric Units - mg/kkg of aluminum product from stationary casting
                         or shot casting
     English Units - Ibs/billion Ibs of aluminum product from
                stationary casting or shot casting
 Acenaphthene
 Benzo(a)anthracene
*Benzo(a)pyrene
 Benzo(ghi)perylene
 Chrysene
 Dibenzo(a,h)anthracene
 Fluoranthene
 Pyrene
 Antimony
 Arsenic
 Cadmium
 Chromium
 Copper
*Fluoride
 Lead
*Nickel
 Selenium
 Zinc

*Regulated Pollutant
    0.000
    0.000
    0.000
    0.000
    0.000
    0.000
    0.000
    0.000
    0.000
    0.000
    0.000
    0.000
    0.000
    0.000
    0.000
    0.000
    0.000
    0.000
       0.000
       0.000
       0.000
       0.000
       0.000
       0.000
       0.000
       0.000
       0.000
       0.000
       0.000
       0.000
       0.000
       0.000
       0.000
       0.000
       0.000
       0.000
                               853

-------
PRIMARY ALUMINUM SUBCATEGORY
SECT - XII
 THIS PAGE INTENTIONALLY LEFT BLANK
                854

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               PRIMARY ALUMINUM SUBCATEGORY   SECT - XIII



                           SECTION XIII

          BEST CONVENTIONAL POLLUTANT CONTROL TECHNOLOGY


EPA  is  not  promulgating best  conventional  pollutant  control
technology  (BCT)  for the primary aluminum subcategory  at  this
time.
                                855

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PRIMARY ALUMINUM SUBCATEGORY   SECT - XIII
THIS PAGE INTENTIONALLY LEFT BLANK
 (Pages  857 and 858 are omitted)
               856

-------
NONFERROUS METALS MANUFACTURING POINT SOURCE CATEGORY
           DEVELOPMENT DOCUMENT SUPPLEMENT
                       for the
       Secondary Aluminum Smelting Subcategory
                  William K. Reilly
                    Administrator
                   Rebecca Hanmer
      Acting Assistant Administrator for Water
              Martha Prothro, Director
      Office of Water Regulations and Standards
            Thomas P. O'Farrell, Director
           Industrial Technology Division
             Ernst .P. Hall, P.E., Chief
               Metals Industry Branch
                         and
              Technical Project Officer
                     May 1989
        U.S. Environmental Protection Agency
                   Office of Water
      Office of Water Regulations and Standards
           Industrial Technology Division
              Washington, D. C.  20460
                         859

-------
860

-------
                SECONDARY ALUMINUM SUBCATEGORY
                        TABLE OF CONTENTS
Section
II
     SUMMARY AND CONCLUSIONS
RECOMMENDATIONS
III  INDUSTRY PROFILE

     Description of Secondary Aluminum Production
     Raw Materials
     Preliminary Treatment
     Smelting and Refining
     Process Wastewater Sources
     Other Wastewater Sources
     Age, Production and Process Profile

IV   SUBCATEGORIZATION

     Factors Considered in Subdividing the Secondary
     Aluminum Subcategory
     Other Factors
     Production Normalizing Parameters

V    WATER USE AND WASTEWATER CHARACTERISTICS

     Wastewater Sources, Discharge Rates and
       Characteristics
     Scrap Drying Wet Air Pollution Control
     Scrap Screening and Milling
     Dross Washing
     Demagging Wet Air Pollution Control
     Delacquering Wet Air Pollution Control
     Ingot Conveyer Casting
     Direct Chill Casting Contact Cooling Water
     Shot Casting Contact Cooling Water
     Stationary Casting Cooling

VI   SELECTION OF POLLUTANTS

     Conventional and Nonconventional Pollutant
       Parameters
     Conventional and Nonconventional Pollutant
       Parameters Selected
     Toxic Pollutants
     Toxic Pollutants Never Detected
     Toxic Pollutants Never Found Above Their
       Analytical Quantification Limit
Page

   867

   871

   889

   889
   889
   889
   891
   893
   894
   894

   901

   901
   901
   903
   903

   905

   906

   909
   909
   909
   909
   910
   910
   910
   911
   911

   943

   944

   944

   945
   945
   945
                               861

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                  SECONDARY ALUMINUM SUBCATEGORY
                         TABLE OF CONTENTS
 Section
 VI
        Toxic Pollutants Present Below Concentrations
          Achievable by Treatment
        Toxic Pollutants Detected in a Small Number
          of Sources
        Toxic Pollutants Selected for Consideration  for
          Establishing Limitations

 VII     CONTROL AND  TREATMENT  TECHNOLOGIES

        Technical Basis of  Existing  Regulations
        Scrap Drying Wet Air  Pollution Control
        Scrap Screening and Milling  Wastewater
        Dross Washing Wastewater
        Demagging Wet Air Pollution  Control
        Delacquering Wet Air Pollution Control
        Ingot Conveyer  Casting Contact Cooling
        Shot  Casting Contact Cooling
        Control and  Treatment Options Considered
        Option A
        Option C
        Control and  Treatment Options Rejected

VIII   COSTS, ENERGY AND NONWATER QUALITY ASPECTS

       Treatment Options Considered
       Option A
       Option C
       Cost Methodology
       Nonwater  Quality Aspects
       Energy Requirements
       Solid Waste
       Air Pollution
IX
X
       BEST PRACTICABLE CONTROL TECHNOLOGY CURRENTLY
       AVAILABLE
Page

   946

   946

   951


   959

   959
   960
   960
   960
   960
   961
   961
   962
   962
   962
   962
   963

   965

   965
   965
   965
   966
   967
   967
   967
   968

  973
       BEST  AVAILABLE TECHNOLOGY ECONOMICALLY  ACHIEVABLE   975

       Technical Approach  to  BAT                           975
       Option A                                             977
       Recycle of Casting  Contact Cooling Water             977
       Recycle of Water Used  in  Wet Air Pollution Control   977
       Option C
                               862

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                SECONDARY ALUMINUM SUBCATEGORY
                        TABLE OF CONTENTS
Section
Page
X    Industry Cost and Pollutant Removal Estimates         978
     Pollutant Removal Estimates                           978
     Compliance Costs                                      979
     BAT Option Selection                                  979
     Wastewater Discharge Rates                            981
     Scrap Drying Wet Air Pollution Control Wastewater     981
     Scrap Screening and Milling                           981
     Dross Washing Wastewater                              981
     Demagging Wet Air Pollution Control                   982
     Delacquering Wet Air Pollution Control                983
     Direct Chill Casting Contact Cooling Water            983
     Ingot Conveyer Casting Contact Cooling Water          984
     Stationary Casting Contact Cooling Water              984
     Shot Casting Contact Cooling Water                    985
     Regulated Pollutant Parameters                        985
     Effluent Limitations                                  986

XI   New Source Performance Standards                      997
     Introduction                                          997
     Technical Approach to BDT                             998
     BDT Option Selection                                  998
     Regulated Pollutant Parameters                        998
     New Source Performance Standards                      999

XII  PRETREATMENT STANDARDS                                1007

     Technical Approach to Pretreatment                    1007
     Pretreatment Standards for Existing and New Sources   1008
     Option A                                              1008
     Option C                                              1008
     Industry Cost and Pollutant Removal Estimates         1009
     PSES and PSNS Option Selection                        1009
     Regulated Pollutant Parameters                        1009
     Pretreatment Standards                                1010

XIII BEST CONVENTIONAL POLLUTANT CONTROL TECHNOLOGY        1025
                               863

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                 SECONDARY ALUMINUM SUBCATEGORY
                          LIST OP TABLES
 Table

 III-l




 III-2


 III-3


 V-l


 V-2


 V-3

 V-4


 V-5


 V-6


 V-7


 V-8


 V-9


 V-10




 V-ll




V-l 2


V-13
      Title
                                             Page
 Initial Operating Year Summary of Plants in      895
 the Secondary Aluminum Subcategory by
 Discharge Type

 Production Ranges for Smelters and Refiners      896
 of the Secondary Aluminum Subcategory

 Summary of Subcategory Processes and             897
Associated Waste Streams

Water Use and Discharge Rates for Scrap Drying   912
Wet Air Pollution Control

Water Use and Discharge Rates for Scrap          913
Screening and Milling
Water Use and Discharge Rates for Dross Washing  914

                                                 915
 Secondary Aluminum Sampling Data - Dross
 Washing Raw Wastewater

 Water  Use and Discharge Rates for                913
 Demagging Wet Air  Pollution Control

 Secondary Aluminum Sampling Data - Demagging      919
 Scrubber Liquor  Raw Wastewater

 Water  Use and Discharge Rates for                923
 Delacquering Wet Air Pollution Control

 Water  Use and Discharge Rates for                924
 Ingot  Conveyer Casting

 Water  Use and Discharge Rates for                925
 Shot Casting

 Secondary Aluminum  Sampling  Data  -  Ingot          926
 Conveyer  Casting Contact Cooling  Water,
 Raw Wastewater

 Secondary  Aluminum  Sampling  Data  -  Demagging      927
 Wet Air Pollution Control and Casting Contact
 Cooling Combined Raw Wastewater

 Secondary Aluminum  Sampling  Data  -  Treatment      929
 Plant Samples, Plant A

 Secondary Aluminum Sampling Data  - Treatment      931
Plant Samples, Plant B
                               864

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i

Table
V-14
V-15
VI-1
VI-2
VIII-1
VIII-2
X-l
X-2
X-3
X-4
XI-1
XI-2
XII-1
XII-2
XII-3
XI I- 4
XII-5
SECONDARY ALUMINUM SUBCATEGORY
LIST OF TABLES
Title Page
Secondary Aluminum Sampling Data - Treatment
Plant Samples, Plant D
Secondary Aluminum Sampling Data - Treatment
Plant Samples, Plant E
Frequency of Occurrence of Toxic Pollutants
Secondary Aluminum Raw Wastewater
Toxic Pollutants Never Detected
Cost of Compliance for the Secondary
Aluminum Subcategory Direct Dischargers
Cost of Compliance for the Secondary
Aluminum Subcategory Indirect Dischargers
Current Recycle Practices Within the Secondary
Aluminum Subcategory
Pollutant Removal Estimates for Secondary
Aluminum Direct Dischargers
Raw Wastewater Discharge Rates for the
Secondary Aluminum Subcategory
BAT Effluent Limitations for the Secondary
Aluminum Subcategory
NSPS Wastewater Discharge Rates for the
Secondary Aluminum Subcategory
NSPS for the Secondary Aluminum Subcategory
Pollutant Removal Estimates for the Secondary
Aluminum Indirect Dischargers
PSES Wastewater Discharge Rates for the
Secondary Aluminum Subcategory
PSNS Wastewater Discharge Rates for the
Secondary Aluminum Subcategory
PSES for the Secondary Aluminum Subcategory
PSNS for the Secondary Aluminum Subcategory



933
936
953
957
970
971
987
988
989
990
1000
1001
1011
1012
1014
1016
1020
865

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Table
III-l
III-2

V-l
V-2
V-3
V-4
V-5
X-l

X-2
       SECONDARY ALUMINUM SUBCATEGORY

                LIST OF FIGURES
       Title
 Secondary Aluminum  Smelting  Process
 Geographic Locations of Secondary Aluminum
 Plants
 Sampling Sites  at Secondary  Aluminum Plant A
 Sampling Sites  at Secondary  Aluminum Plant B
 Sampling Sites  at Secondary  Aluminum Plant C
 Sampling Sites  at Secondary  Aluminum Plant D
 Sampling Sites  at Secondary  Aluminum Plant E
 BAT Treatment Scheme Option  A, Secondary
Aluminum Subcategory
BAT Treatment Scheme Option  C, Secondary
Aluminum Subcategory
Page
    898
    899

    938
    939
    940
    941
    942
    995

    996
                              866

-------
          SECONDARY ALUMINUM SUBCATEGORY
SECT - I
                            SECTION I

                     SUMMARY AND CONCLUSIONS
On  April  8,  1974,  EPA promulgated  technology-based  effluent
limitations  guidelines and standards for the secondary  aluminum
smelting subcategory of the nonferrous metals manufacturing point
source  category.    These  included  BPTf   and  BAT,   effluent
limitations and NSPS  and PSNS (standards).  The purpose of these
effluent limitations and standards was to limit the quantities of
total  suspended  solids,   chemical  oxygen  demand,   fluoride,
ammonia,  aluminum, and copper, and the range of pH discharged in
secondary aluminum smelting wastewaters.   On December 15,  1976,
EPA   promulgated  technology-based  pretreatment  standards  for
existing  sources (PSES) in the secondary  aluminum  subcategory.
The  purpose  of these standards was to limit the  quantities  of
ammonia,  oil  and  grease,  and the range of pH introduced  into
publicly  owned  treatment works in secondary  aluminum  smelting
wastewater discharges.

Under the settlement agreements,  EPA was required to develop BAT
limitations and pretreatment and new source performance standards
for  pollutants  discharged from twenty one  specific  industrial
point  source categories,  including secondary aluminum  smelting
taking into account a specific list of 65 pollutants and  classes
of pollutants.  The list of 65 classes was subsequently clarified
by expanding to a list of 129 specific toxic pollutants. Congress
amended  the Clean Water Act in 1977 to encompass most provisions
of the settlement agreements, including the list of 65 classes of
pollutants.   As  a result of the settlement agreements  and  the
Clean Water Act Amendments, EPA undertook an extensive program to
develop technology-based BAT limitations and pretreatment and new
source standards for the toxic and other pollutants in the twenty
one categories.

EPA promulgated modifications to BAT, NSPS, PSES and PSNS for the
secondary  aluminum subcategory pursuant to the provisions of the
Settlement Agreement and Sections 301,  304,  306, and 307 of the
Clean Water Act and as amended.   Consideration must be given  to
incorporation   of   limits  on  priority  pollutant  levels   in
discharges in these modified standards.  This supplement provides
a  compilation  and analysis of the background material  used  to
develop these effluent limitations and standards.

After promulgation of amendments substantially revising BAT, NSPS
and pretreatment for this subcategory, the Aluminum  Association,
Kaiser Aluminum and Chemical Core., Reynolds Metals Company,  The
Aluminum  Recycling Association, and others filed  petitions  for
review of the amended regulation.
In   November,  1985  the  aluminum  parties  entered  into   two
settlement agreements which resolved issues raised by petitioners
related  to the primary and secondary aluminum subcategories.  T"
                   In
                               867

-------
            SECONDARY ALUMINUM  SUBCATEGORY
SECT - I
 accordance with the settlement agreements, EPA published a notice
 of proposed rulemaking on May 20, 1986 and solicited comments.

 EPA  promulgated  final  amendments for  the  Secondary  Aluminum
 Smelting  Subcategory  on July 7, 1987 (52 FR  25552).  The  flow
 basis  for  two  building  blocks,  ingot  conveyer  casting  and
 demaggxng  wet  air pollution control, were revised  based  on  a
 re-evaluation  of data available in the administrative record  of
 this rulemaking

 The secondary aluminum subcategory is comprised of 47 plants.  Of
 the  47  plants,  10  discharge directly to waters  of  the  U.S.
 (rivers,  lakes,  or  streams);   14 discharge to  publicly  owned
 treatment works (POTW);   and 23 achieve zero discharge of process
 wastewater.                                                ^

 EPA first studied the secondary aluminum subcategory to determine
 whether   differences   in   raw   materials,    final   products,
 manufacturing processes,  equipment,  age and size of plants, water
 usage,   required the development of  separate effluent limitations
 and  standards for  different segments of  the  subcategory.    This
 involved  a  detailed analysis of wastewater discharge and treated
 effluent characteristics,  including  (1) the sources and volume of
 water used,  the processes  used,  and  the sources  of pollutants and
 wastewaters    in the plant;   and   (2)   the    constituents    of
 wastewaters,  including toxic pollutants.

 EPA  also identified several   distinct   control   and   treatment
 technologies   (both  in-plant and end-of-pipe)  applicable  to   the
 secondary  aluminum  subcategory.     The   Agency   analyzed  both
 historical  and newly  generated  data  on the performance of  these
 technologies,   including   their   nonwater   quality  environmental
 impacts   (air   quality impacts and solid  waste  generation)   and
 energy   requirements.   EPA   also studied various  flow   reduction
 techniques  reported  in the  data  collection portfolios  (dcp)   and
 plant visits.

 Engineering  costs  were  prepared for  each of  the   control   and
 treatment  options considered for the   subcategory.   These costs
 were  then  used  by   the  Agency  to   estimate  the  impact   of
 implementing   the various options on the subcategory.   For   each
 control  and   treatment option that the Agency found  to  be   most
 effective  and  technically feasible in  controlling the  discharge
 of  pollutants,  the   number  of potential  closures,   number  of
 employees affected,  and impact on price were  estimated.   These
 results  are   reported in a separate document  entitled  Economic
 Impact  Analysis  of Effluent Limitations and Standards  for  the
 Nonferrous Smelting and Refining Industry (EPA number).

 Based  on  consideration  of  the above  factors,  EPA  identified
 various control and treatment technologies which formed the basis
 for  BPT and selected control and treatment appropriate for  each
 set  of limitations and standards.   The .mass  based,  production
 related limitations and standards for BPT,   BAT,   NSPS,   PSES and
PSNS are presented in Section II.
                               868

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          SECONDARY ALUMINUM SUBCATEGORY
SECT - I
For  BAT,  the  Agency  has  built upon the  BPT  basis  of  lime
precipitation  and  sedimentation by  adding  in-process  control
technologies,   preliminary   treatment   of  ammonia  by   steam
stripping, preliminary treatment of phenolics by activated carbon
adsorption,   and  multimedia  filtration.    In-process  control
technologies  include recycle or reuse of process water from  wet
air pollution control and metal contact cooling.   Filtration  is
added  as an effluent polishing step to further reduce metals and
suspended  solids  concentrations.   To  meet  the  BAT  effluent
limitations  based  on this technology,  the  secondary  aluminum
subcategory is estimated to incur a capital cost of $1.1  million
(1982  dollars)  and  an  annual  cost  of  $0.64  million  (1982
dollars).

The  best demonstrated technology (BDT),  which is the  technical
basis  of  NSPS,  is equivalent to BAT with the addition  of  dry
milling  to  eliminate  the discharge  from  dross  washing.   In
establishing  BDT,  EPA  recognizes  that  new  plants  have  the
opportunity   to   implement   the  best   and   most   efficient
manufacturing  processes and treatment technology.   Treatment of
toxic metals is based upon lime precipitation, sedimentation, and
filtration.  Oil  skimming for the control of oil and grease  and
preliminary treatment of phenolics by activated carbon adsorption
are also included.

Pretreatment standards for existing sources are based on the same
technology  as  BAT.   The technology basis  is  in-process  flow
reduction,   ammonia   steam  stripping  preliminary   treatment,
activated   carbon   adsorption   preliminary   treatment,   lime
precipitation, sedimentation, and multimedia filtration.  To meet
PSES,  the secondary aluminum subcategory  is estimated to incur a
capital  cost of $2.3 million  (1982 dollars) and an annual cost of
$1.4 million  (1982 dollars).

For pretreatment  standards for new sources,  the technology basis
of in-process  flow reduction,  preliminary  treatment, and end-of-
pipe  technology  is  equivalent  to  NSPS.   As  such,  PSNS  are
identical  to NSPS for all waste streams.
                                869

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SECONDARY ALUMINUM SUBCATEGORY
SECT - I
    THIS PAGE  INTENTIONALLY  LEFT BLANK
                    870

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          SECONDARY ALUMINUM SUBCATEGORY
                                       SECT - II
                            SECTION II

                         RECOMMENDATIONS
This  section contains a summary of the effluent limitations  and
standards  which  apply  to the  secondary  aluminum  subcategory
taking  into account the promulgated amendments of March 8,  1984
and July 1, 1987.

1.    EPA  has divided the secondary  aluminum  subcategory  into
nine subdivisions or building blocks for the purpose of  effluent
limitations and standards.  These building blocks are:

     (a)  Scrap drying wet air pollution control,
     (b)  Scrap screening and milling,
     (c)  Dross washing,
     (d)  Demagging wet air pollution control,
     (e)  Delacquering wet air pollution control,
     (f)  Direct chill casting contact cooling,
     (g)  Stationary casting contact cooling,
     (h)   Ingot conveyer casting contact cooling, and
Shot casting contact cooling.
                                                         (i)
2.   EPA  promulgated BPT effluent limitations for the  secondary
     aluminum  subcategory on April 8,  1974,  as Subpart C of 40
     CFR Part 421.  EPA has not promulgated any     modifications
     to   BPT   effluent   limitations.,     The   BPT    effluent
     limitations  apply  to discharges resulting  from  magnesium
                          (demagging  using  either  chlorine  or
                          and wet  residue  processes.   BPT  was
                         on  the performance  achievable  by  the
     application  of  chemical  precipitation  and  sedimentation
     (lime  and settle) technology.   The following BPT  effluent
     limitations were promulgated for existing sources:
removal   processes
aluminum  fluoride)
promulgated  based
      (a)  The  following  limitations establish the  quantity  or
          quality  of pollutants or pollutant  properties,  which
          may  be  discharged  by a point source subject  to  the
          provisions  of  this subpart and which uses  water  for
          metal   cooling,   after   application  of   the   best
          practicable  control  technology  currently  available:
          There   shall  be no discharge  of  process  wastewater
          pollutants  to navigable waters.

      (b)  The  following  limitations establish the  quantity  or
          quality of pollutants or pollutant properties which may
          be  discharged  by  a  point  source  subject  to   the
          provisions  of  this subpart and  which  uses  aluminum
          fluoride  in its magnesium removal process   ("demagging
          process"),           after  application  of  the   best
          practicable  control  technology  currently  available:
          There  shall  be  no discharge  of  process  wastewater
          pollutants to navigable waters.
                                871

-------
           SECONDARY ALUMINUM SUBCATEGORY
                          SECT  -  II
      (c)   The  following  limitations establish the  quantity  or
           quality   of   pollutants   or   pollutant   properties
           controlled by this section,  which may be discharged by
           a  point  source  subject  to the  provisions  of  this
           subpart  and  which  uses  chlorine  in  its  magnesium
           removal   process,   after  application  of  the   best
           practicable control technology currently available:
                                Effluent  Limitations
   Effluent
Characteristic
Average of daily values for 30 consecutive
           days shall not exceed
                   Metric units  (kilograms per 1,000 kg
                                magnesium removed)
                   English units  (Ibs per 1,000 Ibs
                                 magnesium removed)
TSS
COD
pH
                  175
                    6.5
       Within the range of 7.5  to 9.0
                              872

-------
          SECONDARY  ALUMINUM SUBCATEGORY
                         SECT - II
     (d)   The  following  limitations establish the  quantity  or
          quality  of  pollutants or pollutant  properties  which
          may  be  discharged by a point source  subject  to  the
          provisions of this subpart and which processes residues
          by   wet  methods,   after  application  of  the   best
          practical control technology currently available:
                               Effluent Limitations
   Effluent
Characteristic
Average of daily values for 30 consecutive
           days shall not exceed
                   Metric units (kilograms per 1,000 kg
                                of product removed)
                   English units (Ibs per 1,000 Ibs
                                 of product removed)
TSS
Fluoride
Ammonia (as N)
Aluminum
Copper
COD
pH
                    1.5
                    0.4
                    0.01
                    1.0
                    0.003
                    1.0
      Within the range of 7.5 to 9.0
                                873

-------
           SECONDARY ALUMINUM SUBCATEGORY
                 SECT - II
 3.    EPA  is  modifying BAT effluent limitations  to  take  into
       account  the performance achievable by     the  application
       of    chemical   precipitation,   sedimentation,        and
       multimedia   filtration   (lime,   settle,    and    filter)
       technology, along with preliminary treatment consisting  of
       ammonia steam stripping and activated carbon adsorption for
       selected   waste  streams.    The  following  BAT   effluent
       limitations are promulgated for existing sources:

      (a)  Scrap Drying Wet Air Pollution Control

           BAT EFFLUENT LIMITATIONS
    Pollutant or
 Pollutant Property
Maximum  for
Any One  Day
  Maximum  for
Monthly Average
           Metric Units  -  mg/kg  of  aluminum scrap  dried
      English Units  -  Ibs/million Ibs  of  aluminum  scrap  dried
 Lead
 Zinc
 Aluminum
 Ammonia  (as N)
   0.000
   0.000
   0.000
   0.000
     0.000
     0.000
     0.000
     0.000
      (b)   Scrap  Screening and Milling

           BAT EFFLUENT LIMITATIONS
   Pollutant or
Pollutant Property
Maximum for
Any One Day
  Maximum for
Monthly Average
   Metric Units - mg/kg of aluminum scrap screened and milled
    English Units - Ibs/million Ibs of aluminum scrap screened
                            and milled
Lead
Zinc
Aluminum
Ammonia (as N)
   0.000
   0.000
   0.000
   0.000
     0.000
     0.000
     0.000
     0.000
                               874

-------
          SECONDARY ALUMINUM SUBCATEGORY
                 SECT  -  II
     (c)   Dross Washing

          BAT EFFLUENT LIMITATIONS
   Pollutant or
Pollutant Property
 Maximum for
 Any One Day
  Maximum for
Monthly Average
              Metric Units - mg/kg of dross washed
         English Units - Ibs/million Ibs of dross washed
Lead
Zinc
Aluminum
Ammonia (as N)
    3.043
   11.090
   66.410
1,449.000
     1.413
     4.565
    29.450
   636.900
     (d)  Demagging Wet Air Pollution Control

          BAT EFFLUENT LIMITATIONS
   Pollutant or
Pollutant Property
 Maximum for
 Any One Day
  Maximum for
Monthly  Average
            Metric Units  - mg/kg  of  aluminum  demagged
        English Units  -  Ibs/million Ibs  of  aluminum demagged
 Lead
 Zinc
 Aluminum
 Ammonia (as  N)
    0.216
    0.786
    4.711
   102.800
      0.100
      0.324
      2.090
     45.180
      (e)   Delacquering Wet Air Pollution Control

           BAT EFFLUENT LIMITATIONS
    Pollutant or
 Pollutant Property
  Maximum for
  Any One Day
   Maximum for
 Monthly Average
            Metric Units - mg/kg of aluminum delacquered
      English Units - Ibs/million Ibs of aluminum delacquered
 Lead
 Zinc
 Aluminum
 Ammonia (as N)
 Total Phenols
   (4-AAP Method)*

 *At the source
     0.022
     0.082
     0.489
    10.670
     0.001
      0.010
      0.034
      0.217
      4.688
                                875

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           SECONDARY ALUMINUM SUBCATEGORY
                                  SECT - II
       (f)  Direct Chill Casting Contact Cooling

           BAT EFFLUENT LIMITATIONS
    Pollutant or
 Pollutant Property
                  Maximum for
                  Any One Day
   Maximum for
 Monthly Average
               Metric Units - mg/kg of aluminum cast
          English Units - Ibs/million Ibs of aluminum cast
 Lead
 Zinc
 Aluminum
 Ammonia (as N)
                     0.372
                     1.356
                     8.120
                   177.200
      0.173
      0.558
      3.602
     77.880
      (g)    Ingot Conveyer Casting Contact Cooling (When
 Demagging Wet Air Pollution Control is Not Practiced
 Site)
           BAT EFFLUENT LIMITATIONS
                                               Chlorine
                                                   On-
    Pollutant or
 Pollutant Property
                 Maximum for
                 Any One Day
  Maximum  for
Monthly Average
               Metric  Units  -  mg/kg  of  aluminum cast
          English  Units  -  Ibs/million Ibs  of  aluminum cast
 Lead
 Zinc
 Aluminum
 Ammonia (as N)
                    0.019
                    0.068
                    0.409
                    8.931
     0.009
     0.028
     0.182
     3.926
      (h)
Demagging
Site)
Ingot Conveyer Casting Contact Cooling (When  Chlorine
Wet  Air Pollution Control is  Practiced           On-
          BAT EFFLUENT LIMITATIONS
   Pollutant or
Pollutant Property
                 Maximum for
                 Any One Day
  Maximum for
Monthly Average
              Metric Units - mg/kg of aluminum cast
         English Units - Ibs/million Ibs of aluminum cast
Lead
Zinc
Aluminum
Ammonia (as N)
                    0.000
                    0.000
                    0.000
                    0.000
     0.000
     0.000
     0.000
     0.000
                               876

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          SECONDARY ALUMINUM SUBCATEGORY
                SECT - II
     (i)  Stationary Casting Contact Cooling

          BAT EFFLUENT LIMITATIONS
   Pollutant or
Pollutant Property
Maximum for
Any One Day
  Maximum for
Monthly Average
              Metric Units - mg/kg of aluminum cast
         English Units - Ibs/million Ibs of aluminum cast
Lead
Zinc
Aluminum
Ammonia (as N)
   0.000
   0.000
   0.000
   0.000
     0.000
     0.000
     0.000
     0.000
     (j)  Shot Casting Contact Cooling

          BAT EFFLUENT LIMITATIONS
   Pollutant or
Pollutant Property
Maximum for
Any One E>ay
  Maximum for
Monthly Average
              Metric Units - mg/kg of aluminum cast
         English Units - Ibs/million Ibs of aluminum cast
Lead
Zinc
Aluminum
Ammonia (as N)
   0.000
   0.000
   0.000
   0.000
     0.000
     0.000
     0.000
     0.000
                                877

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           SECONDARY  ALUMINUM SUBCATEGORY
                SECT - II
 4.         EPA^   is  modifying   NSPS  based  on   the   performance
           achievable        by    the   application   of    chemical
           precipitation,     sedimentation,       and   multimedia
           filtration  (lime,  settle, and filter)  technology, along
           with preliminary  treatment consisting  of      activated
           carbon  adsorption   and  oil  skimming  for    selected
           waste  streams*    The following effluent standards  are
           promulgated for new sources:

      (a)   Scrap  Drying Wet Air  Pollution Control NSPS
   Pollutant or
Pollutant Property
Maximum for
Any One Day
  Maximum for
Monthly Average
          Metric Units - mg/kg of aluminum scrap dried
     English Units - Ibs/million Ibs of aluminum scrap dried
Lead
Zinc
Aluminum
Ammonia (as N)
Oil and Grease
TSS
pH
   0.000                  0.000
   0.000                  0.000
   0.000                  0.000
   0.000                  0.000
   0.000                  0.000
   0.000                  0.000
     Within the range of 7.0 to 10.0
        at all times
                               878

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          SECONDARY ALUMINUM SUBCATEGORY
                SECT - II
     (b)  Scrap Screening and Milling NSPS
   Pollutant or
Pollutant Property
Maximum for
Any One Day
  Maximum for
Monthly Average
   Metric Units - mg/kg of aluminum scrap screened and milled
    English Units - Ibs/million Ibs of aluminum scrap screened
                            and milled
Lead
Zinc
Aluminum
Ammonia (as N)
Oil and Grease
TSS
PH
     (c)  Dross Washing NSPS

   Pollutant or
Pollutant Property
   0.000                  0.000
   0.000                  0.000
   0.000                  0.000
   0.000                  0.000
   0.000                  0.000
   0.000                  0.000
     Within the range of 7.0 to 10.0
       at all times
Maximum for
Any One Day
  Maximum for
Monthly Average
              Metric Units - mg/kg of dross washed
         English Units - Ibs/million Ibs of dross washed
Lead
Zinc
Aluminum
Ammonia (as N)
Oil and Grease
TSS
pH
   0.000                  0.000
   0.000                  0.000
   0.000                  0.000
   0.000                  0.000
   0.000                  0.000
   0.000                  0.000
    Within the range of 7.0 to 10.0
      at all times
     (d)  Demagging Wet Air Pollution Control NSPS
   Pollutant or
Pollutant Property
Maximum for
Any One Day
  Maximum for
Monthly Average
            Metric Units - mg/kg of aluminum demagged
       English Units - Ibs/million Ibs of aluminum demagged
Lead
Zinc
Aluminum
Ammonia (as N)
Oil and Grease
TSS
pH
   0.216
   0.786
   4.711
 102.800
   7.710
  11.570
     0.100
     0.324
     2.090
    45.180
     7.710
     9.252
     Within the range of 7.0 to 10.0
       at all times
                               879

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           SECONDARY ALUMINUM SUBCATEGORY
                SECT -  II
      (e)   Delacquering  Wet  Air  Pollution  Control  NSPS
    Pollutant  or
 Pollutant  Property
Maximum for
Any One Day
  Maximum for
Monthly Average
           Metric Units  - mg/kg of  aluminum  delacquered
     English  Units  -  Ibs/million  Ibs of aluminum delacquered
Lead
Zinc
Aluminum
Ammonia  (as N)
Total Phenols
   (4-AAP Method)*
TSS
Oil and Grease
pH
*At the source
   0.022
   0.082
   0.489
  10.670
   0.001
     0.010
     0.034
     0.217
     4.688
   1.200                  0.960
   0.800                  0.800
    Within the range of 7.0 to 10.0
      at all times
      (f)  Direct Chill Casting Contact Cooling NSPS
   Pollutant or
Pollutant Property
Maximum for
Any One Day
  Maximum for
Monthly Average
              Metric Units - mg/kg of aluminum cast
         English Units - Ibs/million Ibs of aluminum cast
Lead
Zinc
Aluminum
Ammonia (as N)
Oil and Grease
TSS
pH
   0.372                  0.173
   1.356                  0.558
   8.120                  3.602
 177.200                 77.880
  13.290                 13.290
  19.940                 15.950
     Within the range of 7.0 to 10.0
       at all times
                               880

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          SECONDARY ALUMINUM SUBCATEGORY
                SECT - II
     (g)   Ingot  Conveyer  Casting Contact  Cooling  NSPS  (When
Chlorine   Demagging   Wet   Air   Pollution   Control   is   Not
Practiced On-Site)
   Pollutant or
Pollutant Property
Maximum for
Any One Day
  Maximum for
Monthly Average
              Metric Units - mg/kg of aluminum cast
         English Units - Ibs/million Ibs of aluminum cast
Lead
Zinc
Aluminum
Ammonia (as N)
TSS
Oil and Grease
PH
   0.019                  0.009
   0.068                  0.028
   0.409                  0.182
   8.931                  3.926
   1.005                  0.804
   0.670                  0.670
    Within the range of 7.0 to 10.0
      at all times
      (h)   Ingot  Conveyer  Casting Contact  Cooling  NSPS   (When
Chlorine    Demagging    Wet    Air    Pollution    Control    is
Practiced On-Site)
   Pollutant or
Pollutant Property
Maximum  for
Any One  Day
  Maximum  for
Monthly Average
              Metric Units - mg/kg of aluminum  cast
         English Units  -  Ibs/million Ibs of aluminum  cast
 Lead
 Zinc
 Aluminum
 Ammonia  (as  N)
 TSS
 Oil and  Grease
 pH
    0.000                   0.000
    0.000                   0.000
    0.000                   0.000
    0.000                   0.000
    0.000                   0.000
    0.000                   0.000
     Within the range of 7.0 to 10.0
       at  all times
                                881

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           SECONDARY ALUMINUM SUBCATEGORY
                 SECT  -  II
      (i)  Stationary Casting Contact Cooling NSPS
    Pollutant or
 Pollutant Property
Maximum for
Any One Day
  Maximum  for
Monthly Average
               Metric Units - mg/kg of aluminum cast
          English Units - Ibs/million Ibs of aluminum cast
 Lead
 Zinc
 Aluminum
 Ammonia  (as  N)
 Oil  and  Grease
 TSS
 PH
    0.000
    0.000
    0.000
    0.000
    0.000
    0.000
     0.000
     0.000
     0.000
     0.000
     0.000
     0.000
     Within the range of 7.0 to 10.0
       at all times
      (j)  Shot Casting Contact Cooling NSPS
   Pollutant or
Pollutant Property
Maximum for
Any One Day
  Maximum for
Monthly Average
              Metric Units - mg/kg of aluminum cast
        English Units - Ibs/million Ibs of aluminum cast
Lead
Zinc
Aluminum
Ammonia (as N)
Oil and Grease
TSS
PH
   0.000                  0.000
   0.000                  0.000
   0.000                  0.000
   0.000                  0.000
   0.000                  0.000
   0.000                  0.000
     Within the range of  7.0  to 10.0
       at all times
5.   EPA  is  modifying PSES based on the performance  achievable
     by the application of chemical precipitation, sedimentation,
     and  multimedia  filtration  (lime,   settle,   and  filter)
     technology,  along with preliminary treatment consisting  of
     ammonia  steam stripping and activated carbon adsorption for
     selected   waste   streams.     The   following   mass-based
     pretreatment standards are promulgated for existing sources:
                               882

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          SECONDARY ALUMINUM SUBCATEGORY
                 SECT - II
     (a)  Scrap Drying Wet Air Pollution Control PSES
   Pollutant or
Pollutant Property
 Maximum for
 Any One Day
  Maximum for
Monthly Average
          Metric Units - mg/kg of aluminum scrap dried
     English Units - Ibs/million Ibs of aluminum scrap dried
Lead
Zinc
Ammonia (as N)
    0.000
    0.000
    0.000
     (b)  Scrap Screening and Milling PSES
   Pollutant or
Pollutant Property
 Maximum for
 Any One Deiy
     0.000
     0.000
     0.000
  Maximum for
Monthly Average
   Metric Units - mg/kg of aluminum scrap screened and milled
    English Units - Ibs/million Ibs of aluminum scrap screened
                            and milled
Lead
Zinc
Ammonia (as N)
    0.000
    0.000
    0.000
     0.000
     0.000
     0.000
     (c)  Dross Washing PSES

   Pollutant or
Pollutant Property
 Maximum for
 Any One Day
  Maximum for
Monthly Average
              Metric Units - mg/kg of dross washed
         English Units - Ibs/million Ibs of dross washed
Lead
Zinc
Ammonia (as N)
    3.043
   11.090
1,449.000
     1.413
     4.565
   636.000
     (d)  Demagging Wet Air Pollution Control PSES
   Pollutant or
Pollutant Property
 Maximum for
 Any One Day
  Maximum for
Monthly Average
            Metric Units - mg/kg of aluminum demagged
       English Units - Ibs/million Ibs of aluminum demagged
Lead
Zinc
Ammonia (as N)
    0.216
    0.786
  102.800
     0.100
     0.324
    45.180
                               883

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          SECONDARY ALUMINUM SUBCATEGORY
                SECT - II
      (e)  Delacquering Wet Air Pollution Control PSES
   Pollutant or
Pollutant Property
Maximum for
Any One Day
  Maximum for
Monthly Average
           Metric Units - mg/kg of aluminum delacquered
     English Units - Ibs/million Ibs of aluminum delacquered
Lead                           0.022
Zinc                           0.082
Ammonia  (as N)                10.670
Total Phenols                  0.001
   (4-AAP Method)*

*At the source

     (f)  Direct Chill Casting Contact Cooling PSES
                          0.010
                          0.034
                          4.688
   Pollutant or
Pollutant Property
Maximum for
Any One Day
  Maximum for
Monthly Average
              Metric Units - mg/kg of aluminum cast
        English Units - Ibs/billion Ibs of aluminum cast
Lead
Zinc
Ammonia (as N)
   0.372
   1.356
 177.200
     0.173
     0.558
    77.800
     (g)   Ingot  Conveyer  Casting Contact  Cooling  PSES  (When
Chlorine   Demagging   Wet   Air   Pollution   Control   is   Not
Practiced On-Site)
   Pollutant or
Pollutant Property
Maximum for
Any One Day
  Maximum for
Monthly Average
              Metric Units - mg/kg of aluminum cast
         English Units - Ibs/million Ibs of aluminum cast
Lead
Zinc
Ammonia (as N)
   0.019
   0.068
   8.931
     0.009
     0.028
     3.926
                               884

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          SECONDARY ALUMINUM SUBCATEGORY
                SECT - II
     (h)   Ingot  Conveyer  Casting Contact  Cooling  PSES  (When
Chlorine    Demagging    Wet    Air    Pollution    Control    is
Practiced On-Site)
   Pollutant or
Pollutant Property
Maximum for
Any One Day
  Maximum for
Monthly Average
              Metric Units - mg/kg of aluminum cast
         English Units - Ibs/million Ibs of aluminum cast
Lead
Zinc
Ammonia (as N)
   0.000
   0.000
   0.000
     0.000
     0.000
     0.000
     (i)  Stationary Casting Contact Cooling PSES
   Pollutant or
Pollutant Property
Maximum for
Any One Day
  Maximum for
Monthly Average
              Metric Units - mg/kg of aluminum cast
        English Units - Ibs/million Ibs of aluminum cast
Lead
Zinc
Ammonia (as N)
   0.000
   0.000
   0.000
   (j)  Shot Casting Contact Cooling PSES
   Pollutant or
Pollutant Property
Maximum for
Any One Day
     0.000
     0.000
     0.000
  Maximum for
Monthly Average
              Metric Units - mg/kg of aluminum cast
        English Units - Ibs/million Ibs of aluminum cast
Lead
Zinc
Ammonia  (as N)
   0.000
   0.000
   0.000
     0.000
     0.000
     0.000
7.   EPA  is  modifying PSNS based on the performance  achievable
     by the application of chemical precipitation, sedimentation,
     and  multimedia  filtration   (lime,   settle,   and  filter)
     technology,  along with preliminary treatment consisting  of
     activated  carbon  adsorption for the delacquering  wet  air
     pollution  control waste stream.   The following  mass-based
     pretreatment standards are promulgated for new sources:
                                885

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           SECONDARY ALUMINUM SUBCATEGORY
                 SECT - II
       (a)  Scrap Drying Wet Air Pollution Control PSNS
    Pollutant or
 Pollutant Property
 Maximum for
 Any One Day
   Maximum for
 Monthly Average
            Metric Units - mg/kg of aluminum scrap dried
      English Units - Ibs/million Ibs of aluminum scrap dried
 Lead
 Zinc
 Ammonia (as N)
    0.000
    0.000
    0.000
      (b)  Scrap Screening and Milling PSNS
    Pollutant or
 Pollutant Property
 Maximum for
 Any One Day
      0.000
      0.000
      0.000
   Maximum for
 Monthly Average
    Metric Units - mg/kg of aluminum scrap screened and milled
     English Units - Ibs/million Ibs of aluminum scrcip screened
                             and milled
 Lead
 Zinc
 Ammonia (as  N)
    0.000
    0.000
    0.000
      (c)   Dross  Washing  PSNS
    Pollutant  or
Pollutant  Property
Maximum for
Any One Day
      0.000
      0.000
      0.000
  Maximum for
Monthly Average
              Metric Units - mg/kg of dross washed
         English Units -  Ibs/million Ibs of dross washed
Lead
Zinc
Ammonia  (as N)
   0.000
   0.000
   0.000
     0.000
     0.000
     0.000
      (d)  Demagging Wet Air Pollution Control PSNS
   Pollutant or
Pollutant Property
Maximum for
Any One Day
  Maximum for
Monthly Average
            Metric Units - mg/kkg of aluminum demagged
       English Units - Ibs/billion Ibs of aluminum demagged
Lead
Zinc
Ammonia (as N)
   0.216
   0.786
 102.800
     0.100
     0.324
    45.180
                               886

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          SECONDARY ALUMINUM SUBCATEGORY
                SECT - II
     (e)  Delacquering Wet Air Pollution Control PSNS
   Pollutant or
Pollutant Property
Maximum for
Any One Day
  Maximum  for
Monthly Average
           Metric Units - mg/kg of aluminum delacquered
     English Units - Ibs/million Ibs of aluminum delacquered
Lead
Zinc
Ammonia (as N)
Total Phenols
  (4-AAP Method)*
   0.022
   0.082
  10.670
   0.001
      0.010
      0.034
      4.688
*At the source

     (f)  Direct Chill Casting Contact Cooling PSNS
   Pollutant or
Pollutant Property
Maximum for
Any One Day
   Maximum for
 Monthly Average
              Metric Units - mg/kg of aluminum cast
        English Units - Ibs/million Ibs of aluminum cast
Lead
Zinc
Ammonia (as N)
   0.372
   1.356
 177.200
      0.173
      0.558
     77.880
     (g)   Ingot  Conveyer  Casting Contact  Cooling  PSNS
Chlorine   Demagging   Wet   Air   Pollution   Control   is
Practiced On-Site)
                                 (When
                                  Not
   Pollutant or
Pollutant Property
Maximum for
Any One Day
   Maximum for
,Monthly Average
             mg/kg  (Ib/million Ibs) of aluminum cast
Lead
Zinc
Ammonia  (as N)
    0.019
    0.068
    8.931
      0.009
      0.028
      3.926
                                887

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           SECONDARY ALUMINUM SUBCATEGORY
                 SECT - II
      (h)   Ingot  Conveyer  Casting Contact  Cooling  PSNS  (When
 Chlorine    Demagging    Wet    Air    Pollution    Control    is
 Practiced On-Site)
    Pollutant or
 Pollutant Property
 Maximum for
 Any One Day
   Maximum for
 Monthly Average
                    (Ib/million Ibs) of aluminum cast
 Lead
 Zinc
 Ammonia (as N)
    0.000
    0.000
    0.000
      0.000
      0.000
      0.000
      (i)   Stationary Casting Contact Cooling PSNS
    Pollutant  or
 Pollutant  Property
Maximum for
Any One Day
  Maximum for
Monthly Average
              Metric  Units  -  mg/kg  of  aluminum cast
         English  Units -  Ibs/million Ibs  of  aluminum  cast
Lead
Zinc
Ammonia  (as N)
   0.000
   0.000
   0.000
      (j)  Shot Casting Contact Cooling PSNS
   Pollutant or
Pollutant Property
Maximum for
Any One Day
     0.000
     0.000
     0.000
  Maximum for
Monthly Average
              Metric Units - mg/kg of aluminum cast
        English Units - Ibs/million Ibs of aluminum cast
Lead
Zinc
Ammonia (as N)
   0.000
   0.000
   0.000
     0.000
     0.000
     0.000
                               888

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         SECONDARY ALUMINUM SUBCATEGORY
SECT - III
                           SECTION III

                         INDUSTRY PROFILE
This  section of the Secondary Aluminum Supplement describes  the
raw  materials and processes used in producing recycled  aluminum
and   presents  a  profile  of  the  secondary  aluminum   plants
identified in this study.

DESCRIPTION OF SECONDARY ALUMINUM PRODUCTION

Secondary  aluminum production involves two basic process  steps:
pretreatment  and smelting and refining.   A pretreatment step is
required  before  smelting and refining operations can  be  under
taken because this industry uses scrap aluminum (much of which is
contaminated)  for its raw material.   The two  processes,  their
components,  and  variations are discussed below.   Figure  III-l
(page  898) represents a general flow diagram of the two  process
steps.

RAW MATERIALS

The secondary aluminum subcategory uses aluminum-bearing scrap to
produce metallic aluminum and aluminum alloys.  Much of the scrap
used is purchased from scrap dealers of industrial plants.  There
are  six  primary classifications of scrap  processed:   aluminum
cans, old sheet and castings, new clippings and forgings, borings
and turnings, residues, and high iron.

New  scrap  is  produced during the  manufacture  of  a  finished
product  and  originates  from the  aircraft  industry,  aluminum
formers,  and other manufacturing plants.   Old scrap (sheet  and
castings) is comprised of worn out,  damaged or obsolete articles
and  includes  automobile parts,  household items,  and  airplane
parts.  Borings and turnings are by-products of the machining  of
castings,  rods,  and  forgings  by the aircraft  and  automobile
industry. Residues- consist of drosses, skimmings, and slags which
are  obtained from primary reduction plants,  secondary  smelting
plants,  casting  plants,  and  foundries.   Foil from  discarded
packaging  constitutes  a minor source of raw material  for  this
subcategory.   High iron aluminum scrap which is to be reused  in
the   secondary  aluminum  subcategory  require  more   extensive
treatment   before  smelting  than  other  classifications  scrap
aluminum.

PRELIMINARY TREATMENT

Preliminary  treatment of scrap involves preparing  the  material
for further processing and removing contaminants.  As Figure III-
1   (page  898) indicates, the scrap pretreatment  process  varies
depending  on the source and type of raw material being  handled.
There   is  also  variation  in  the  degree  to  which  scrap  is
pretreated among facilities.  There are three general methods  of
                               889

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           SECONDARY ALUMINUM  SUBCATEGORY
SECT - III
 pretreating:       mechanical,      hydro-metallurgical,       and
 pyrometallurgical,  with the method used being dependent  on  the
 type  of  scrap.  The mechanical method  involves  shredding  and
 classifying,     baling,    and    milling     and     screening.
 Hydrometallurgical  treatment involves leaching with  water,  and
 pyrometallurgical  processing  involves burning and  drying,  and
 sweating.   Depending on the type of raw  material,  pretreatment
 may consist of a combination of these methods before smelting and
 refining is effected.

 Old sheet,  castings,  and clippings preparation is a dry process
 that can vary from no pretreatment to crushing and screening that
 compacts the scrap.   New clippings and forgings usually  require
 little^  preparation  other than sorting;  however,  they  may  be
 contaminated  with  cutting oils,  and may require  crushing  and
 drying  to  remove the oils.   Can scrap is often  pretreated  by
 burning the lacquer from the cans prior to smelting or remelting.
 Organic  fumes  emitted during this process are an air  pollution
 source.   Wet scrubbers are normally chosen over afterburners  and
 baghouses  to  control emissions because of the explosion  hazard
 that  exists.   Cable,  which is not considered a major source  of
 aluminum  scrap requires shredding and classifying to remove  the
 insulation  and ferrous portions from the aluminum.   The  borings
 and  burnings   are also often contaminated by  cutting  oils  and
 require  burning or drying to remove that contaminant.   The entire
 procedure  consists  of (1)  crushing the borings and  turnings  to
 compact  the  scrap,   (2)  heating the scrap in an oil or  gas-fired
 rotary dryer to remove organic material and water,   (3)  screening
 to remove aluminum fines,  and (4)  magnetically removing  the  tramp
 iron.

 Aluminum  and  other metals  from junked  automobiles are  recovered
 in  a  water elutriator  system where scrap  auto  body  parts  are
 separated from  light  waste materials  based on specific   gravity
 differences.    Water,   or other  flotation media,   flow upward and
 separate the lightweight materials  from the metal which  continues
 to sink.   Metal  collected at  the  bottom of the system is  removed
 with   a  perforated conveyer,  and  the water  drains  into a   holding
 tank for settling and  then returns  to the system.

 Residues, such  as drosses, skimmings, and slags, contain 10  to 30
 percent  aluminum,  as well as oxides, carbides, nitrides,  fluxing
 salts,    and  other  contaminants.    Metallic  aluminum   can  be
 liberated  from the impurities using either  dry or wet processes.
 The  dry process consists of  milling,  screening,  and  magnetic
 separation   for iron removal.   The wet process involves   milling
 and  leaching with water to  remove the contaminants.   The washed
 material  is  then screened,  dried,  and passed  through a magnetic
 separator.   Heavy  metallic skims,  a minor source of  aluminum,
 require  little pretreatment.

Foil,  which  is  another  minor source of  raw material  for  the
subcategory, is usually pretreated by roasting to remove paper or
wax  backings.    High  iron content scrap often is  subjected  to
sweating treatment to remove impurities.   This process  involves
                               890

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         SECONDARY ALUMINUM SUBCATEGORY
SECT - III
placing  the  iron-contaminated aluminum in a  sweating  furnace.
This  furnace has sloped sides and the molten aluminum flows down
the  slope,  leaving the higher melting point materials  such  as
iron  behind.   Alternately,  the  high  iron scrap also  can  be
purified by crushing it and removing the iron magnetically.

SMELTING AND REFINING

The  second step of the manufacturing process for  the  secondary
aluminum  subcategory  is  smelting  and  refining.    This  step
actually  consists  of  five substepss   charging  scrap  to  the
furnace; addition of fluxing agents; addition of alloying agents;
demagging or degassing; and skimming.

Charging  of  scrap into the furnace can be a batch process or  a
continuous process.   Each cycle,  called a "heat",  will vary in
length  depending  on  the process.   Charging  wells  are  often
designed to permit the introduction of chips and scrap below  the
surface  of  a  previously melted charge called a  "heel."   This
design  not  only  minimizes oxidation,  but  provides  for  more
efficient application of pollution control systems.

The  next  step  is fluxing the molten  charge.   There  are  two
general  types of fluxes:   cover fluxes that are used to  reduce
oxidation of the melt by air,  and solvent fluxes that react with
contaminants such as nonmetallics, residues from burned coatings,
and  dirt  to form insolubles which float on the surface  of  the
melt as slag.

Next,  alloying  agents are added to the melt in varying  amounts
according  to  production   specifications.    Copper,   silicon,
manganese,  or zinc are typical alloys added.  Mixing the furnace
contents is necessary to assure uniform composition.  Nitrogen or
other  inert  gases  may  be  injected  to  aid  in  the  mixing.
Magnesium  is  another  alloying  agent  used.    However,  scrap
aluminum,  received  by the secondary aluminum smelters  averages
about  0.3  to 0.5 percent magnesium,  while the product line  of
alloys produced averages about 0.1 percent.  Therefore, after the
furnace  is fully charged and the melt brought up to the  desired
chemical  specification,  it is usually necessary to  remove  the
excess magnesium (known as "demagging").

Demagging  is accomplished with chlorine or chlorinating  agents,
such  as  anyhdrous aluminum chloride or with aluminum  fluoride.
Magnesium chloride or magnesium fluoride is formed and  collected
in  the  fluxing  agents  on top of  the  molten  melt.   As  the
magnesium  is  depleted,  chlorine will consume aluminum and  the
excess aluminum chloride or aluminum fluoride present volatilizes
into the surrounding air and is a source of air pollution.

Magnesium  is  the only metal removable from the  alloy  in  this
manner.   Other  metal  alloy  levels  must be  adjusted  by  the
addition of either more aluminum (dilution) or more of the metal.

Chlorination  is performed at temperatures between 760 and 815°C.
                               891

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           SECONDARY  ALUMINUM  SUBCATEGORY
SECT - III
 As  a   rule  of  thumb,   the  reaction  requires   3.5  kilograms  of
 chlorine per kilogram of magnesium  removed.   Elemental  chlorine
 gas  is fed under pressure through  tubes or lances to the  bottom
 of  the  melt.   As it bubbles through the melt,  it reacts  with
 magnesium and aluminum to form chlorides, which float to the melt
 surface  where   they  combine  with the fluxing  agents  and  are
 skimmed  off.    Because magnesium   is  above  aluminum  in  the
 electromotive  series,   aluminum chloride will be reduced by  anv
 available  magnesium  in the melt.   At  the  beginning  of  the
 demagging  cycle,  the   principal reaction product  is  magnesium
 chloride.   As  magnesium is removed and there is less  available
 for ^reaction  with  chlorine,  the  reaction  of  chlorine  with
 aluminum becomes more significant,  the reduction of the aluminum
 chloride by magnesium becomes less likely,  and the production of
 aluminum chloride, a volatile compound, becomes significant.   The
 aluminum _chloride  escapes and considerable fuming results  from
 the chlorination,  making ventilation and air pollution equipment
 necessary.    Control  of fumes is frequently accomplished by  wet
 scrubbing and,  thus, is a source of water contamination.

 Aluminum fluoride as a demagging agent reacts with the  magnesium
 to form magnesium fluoride,   which in turn combines with the  flux
 on top of the melt,   where it is skimmed off.   In practice,  about
 4.3  kilograms  of aluminum fluoride are required per  kilogram  of
 magnesium  removed.     The  air   contaminants  exist   as   gaseous
 fluorides or  as fluoride dusts and are a source of air  pollution.
 The fluorides are controlled by  either dry or  wet  methods.    When
 dry scrubbing  is used,   a solid waste is   generated.   When   wet
 scrubbing   is   used,   both  water pollution and solid   waste   are
 generated.

 Some   facilities   in the  secondary aluminum subcategory   are   not
 limited  by a magnesium  content in their  product, particularly the
 deoxidant  manufacturers, and   they  make  no  attempt   to  remove
 magnesium.  Therefore,  these  plants  do not  generate the magnitude
 of  fumes produced by demagging,   and as a  result,  do not require
 extensive  air  pollution control  equipment   and  related  water
 usage.
In  the skimming step,   the dross or slag,  with
impurities, is skimmed from the molten aluminum.
is  stored  for shipment to a  residue  processor,
discarded.
      its  associated
      The cooled slag
        recycled,   or
The ^product  line(s)  of  each smelter  can  be  categorized  as
specification  alloy ingots,  billets,  hot metal,  notched  bar,
shot, _  and  hardeners.   Specification  alloy  ingots,  used  by
foundries  for  casting,  are the most important products of  the
secondary aluminum subcategory.   Cooling can be done with either
contact  or  noncontact cooling water,  and air cooling  is  also
USfv j    In9ot conveyer casting is the most predominant  casting
method  used  in  the  secondary  aluminum  subcategory.   Molten
aluminum  is  poured  into ingot molds traveling  on  a  conveyer
system._   The  aluminum is allowed to briefly air cool  prior  to
contacting  the metal surface and mold with water.   This  allows
                               892

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         SECONDARY ALUMINUM SUBCATEGORY
                                        SECT - III
the  metal surface to solidify so that the aluminum surfaces  are
not water marked.  Enough heat is extracted from the aluminum  for
solidification  and  to  prevent breaking when  the  aluminum  is
removed  from the  mold. Notched bar,  RAI, and redox  casting  are
three variations of ingot conveyer casting.

Direct    chill   casting   is   characterized   by    continuous
solidification  of  the  metal while  it  is  being  poured.   The
length  of an ingot cast using this method is determined  by  the
vertical  distance  it  is allowed to drop rather  than  by  mold
dimensions.   Molten  aluminum is tapped from the melting furnace
and  flows  through a distributor channel into  a  shallow  mold.
Noncontact  cooling  water circulates within this  mold,  causing
solidification of  the aluminum.  The  base of the mold is attached
to  a  hydraulic cylinder which is gradually lowered  as  pouring
continues.   As  the solidified aluminum leaves the mold,  it  is
sprayed  with contact cooling water to reduce the temperature  of
the forming ingot.  The cylinder continues to descend into a tank
of water, causing  further cooling of  the ingot as it is immersed.
When the cylinder  has reached its lowest position,  pouring stops
and the ingot is lifted from the pit.   The hydraulic cylinder is
then raised and positioned for another casting cycle.

Plants  using  contact  cooling water  recycle  systems  generate
intermittent   discharges  (accompanied  with  sludge   removal).
Billets,  manufactured  for use in extrusion plants,  are  cooled
with   noncontact water that is recycled.   Sometimes the  molten
metal is poured directly into preheated crucibles,  then  shipped
while  still in a molten form.   No water  is used.   Notched  bar
molds  may  be  air  or  water  cooled  with  either  contact  or
noncontact water.

Aluminum  shot is also used as a deoxiclant in the steel industry.
Molten metal is poured into a vibrating feeder, where droplets of
molten  metal  are   formed  through  perforated  openings.    The
droplets  are  cooled  in a  quench  tank.   Water  is  generally
recycled, and periodic sludge removal is  required.

PROCESS WASTEWATER SOURCES

The  primary areas of  water use and wastewater production  in  the
secondary aluminum subcategory are as follows:
      Scrap drying wet air pollution control,
      Scrap screening and milling,
      Dross washing,
      Demagging wet air pollution control,
      Delacquering wet air pollution control,
      Direct chill casting contact cooling water,
        Ingot conveyer casting  contact cooling,     8.    Stationary
 casting  contact  cooling water, and  9.   Shot  casting   contact
 cooling water.
1,
2,
3.
4,
5
6
7
                                893

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          SECONDARY ALUMINUM  SUBCATEGORY
SECT - III
OTHER WASTEWATER  SOURCES

There are  other wastewater  streams associated with the production
of  secondary aluminum.  These  include but are not limited to:

  1.  Maintenance and cleanup  water, and
  2.  Stormwater  runoff.

These  wastewaters are not  considered as part of this rulemaking.
EPA believes  that the flows  and pollutant  loadings  associated
with  these streams are insignificant relative to the  wastewater
streams selected,  or are best handled by the appropriate  permit
authority  on a case-by-case basis under the authority of Section
402 of the CWA.

AGE, PRODUCTION,  AND PROCESS PROFILE

Figure  III-2  (page  899)  shows the location  of  47  secondary
aluminum reduction plants.  Most of the plants are located in the
eastern  United   States,  and  most are in urban  areas  near  raw
materials and markets.  The notations within the states indicated
the  type of discharge the  facilities use,  direct (D),  indirect
(I), or zero (Z).

The data in Table III-l (page  895) indicate that the majority  of
facilities  (34)  are  less than 35  years  old,  reflecting  the
relatively recent development  of this industry.

In addition, most facilities practice zero discharge with only 21
percent (10 facilities) discharging directly to waters of the U.S.

The  data in Table III-2 (page 896) indicate that the majority of
facilities  produce  between   5,000 and 20,000 kkg  per  year  of
secondary aluminum.   Table III-3 (page 897)  provides a summary of
the  plants having the various secondary aluminum processes;   the
number of plants generating wastewater from the processes is also
shown.
                               894

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SECONDARY ALUMINUM SUBCATEGORY
SECT - III



















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                   895

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SECONDARY ALUMINUM SUBCATEGORY    SECT - III
                  TABLE III-2

  PRODUCTION RANGES FOR SMELTERS AND REFINERS
     OF THE SECONDARY ALUMINUM SUBCATEGORY
                   (kkg/yr)
 Production Ranges

      0 - 2500

   2501 - 5000

   5001 - 10000

  10000 - 20000

  20001 - 30000

  30000 - 4-

  No Data

  Total Number of
  Plants in Survey
Number of Plants

     4

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    16-

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     3

     3

     6

    47
                     896

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         SECONDARY ALUMINUM SUBCATEGORY
               SECT - III
                           TABLE II1-3

  SUMMARY OF SUBCATEGORY PROCESSES AND ASSOCIATED WASTE STREAMS
        Process
Raw Material Preparation
  Number of
Plants With
  Process
   Scrap drying air pollution      23
   control

   Scrap screening and milling     18

   Dross washing                    3

   Dust air pollution control      13

Delacquering                        5

   air pollution control            5


Demagging

   air pollution- control          17

Casting                           40

   Ingot conveyer casting         14

   Shot casting                    4
Number of Plants
   Generating
   Wastewater
                      1

                      3

                      0
                     17



                     14

                      4
                               897

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SECONDARY ALUMINUM SUBCATEGORY     SECT  - III
                  ALUMINUM SCRAP
  SHIP MOLTEN ALUMINUM     SHIP ALUMINUM INGOTS
               Figure  III-1




 SECONDARY ALUMINUM  SMELTING  PROCESS
                   898

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SECONDARY ALUMINUM SUBCATEGORY
SECT  -  III
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-------
SECONDARY ALUMINUM SUBCATEGORY
SECT - III
      THIS PAGE INTENTIONALLY LEFT BLANK
                      900

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          SECONDARY ALUMINUM SUBCATEGORY
                                  SECT - IV
                            SECTION IV

                        SUBCATEGORIZATION
This  section  summarizes  the  factors  considered  during   the
designation of the secondary aluminum subcategory and its related
subdivisions. Secondary aluminum was identified as a  subcategory
in a final regulation promulgated in 1974 and BPT, BAT, NSPS, and
PSNS effluent limitations and standards were established for  the
secondary  aluminum subcategory. The purpose of this study is  to
support modifications to the BAT, NSPS, and PSNS regulations.
FACTORS
CONSIDERED  IN  SUBDIVIDING  THE
SECONDARY
ALUMINUM
SUBCATEGORY
The  factors  for general subcategorization were  each  evaluated
when  establishing  the secondary aluminum  subcategory  and  its
subdivisions.   In the discussion that follows, the factors  will
be  described  as they pertain to  this  particular  subcategory.
Subcategorization  of the entire nonferrous metals  industry  and
evaluation  of the factors used in this process are discussed  in
Section IV of the General Development Document.

The  rationale  for dividing the secondary  aluminum  subcategory
into  segments  or  building blocks considers  the  diversity  in
source  of  raw  materials,  the  use  of  certain  manufacturing
processes  by  only  a few facilities,  and  the  differences  in
available  technologies  for  final  product  processing   (i.e.,
contact  cooling  water,  air  cooling,  and  noncontact  cooling
water).

The  raw materials used by secondary aluminum plants  are  either
solid scraps (clippings and forgings,  borings and turnings,  and
old  sheet and castings) or residues from aluminum reduction  and
smelting.   Since all secondary smelters use the various types of
scraps  at one time or another,  the type of scrap cannot be used
as  a basis for subcategorization.   However,  many  plants  have
scrap drying operations.   Most of these plants use air pollution
control devices in this process.   A few plants use wet scrubbers
which  produce  wastewater.   Some facilities also use  water  in
scrap screening and milling,  generating wastewater.   Therefore,
scrap  drying  wet air pollution control and scrap screening  and
milling should be considered segments.

Can scrap is normally heated prior to melting to burn the lacquer
contained  on  the  cans.   Wet scrubbers are  normally  used  to
control  air  pollution  rather than afterburners  and  baghouses
because  of  the  explosion  hazard.    Explosion  potential   is
increased  if  the scrap is shredded due to aluminum  fines  that
would collect in dry scrubbing systems.   Five plants operate wet
scrubbers, indicating that delacquering wet air pollution control
should be considered a segment.
                               901

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          SECONDARY ALUMINUM SUBCATEGORY
SECT - IV
Furnace  residue  processing to recover aluminum  can  produce  a
wastewater stream with treatable pollutant concentrations.   Five
facilities process furnace residues,  and four of these use water
for  the processing.   Since this process produces a  potentially
contaminated waste stream it has been identified as a segment.

Plants  practicing  magnesium removal (demagging),  use either  a
chlorine  or aluminum fluoride process.   The  demagging  process
requires  air pollution control devices to minimize fuming.   Wet
scrubbing  can be practiced with both types of demagging and  the
resulting scrubber water is usually treated by pH adjustment  and
settling.

Thirty-four  plants  demag,  20  generate  wastewater  from  fume
scrubbing.    Because   the  demagging  process  can  produce   a
contaminated  wastewater,  it  has been identified as  a  segment
within the secondary aluminum subcategory.

The  final  secondary  aluminum process  s.tep  is  casting.   The
technique  for  cooling the aluminum into various  shapes  varies
within the subcategory and with the product.   Air cooling, water
contact cooling, and water noncontact cooling are all used.  When
water  contact cooling is used,  the cooling water is  frequently
recycled.   However,  a  blowdown  stream  may  be  necessary  to
dissipate the build-up of dissolved solids.  This blowdown stream
may  have,  in addition to treatable dissolved  solids,  oil  and
grease and phenolics, depending on whether lubricants are used in
casting.  This manufacturing process has also been considered  to
be segment within the secondary aluminum subcategory.

Within  the  secondary  aluminum subcategory the  processes  that
produce the wastewaters discussed previously,  residue processing
wastewater,  demagging fume scrubber liquors, and contact cooling
water,  are not all present at all facilities.   Some  facilities
may  have one,  others combinations of two,  and still others all
three.   The  building  block approach used  in  this  regulation
accommodates  these differences by establishing  limitations  and
standards for each wastewater stream.
Limitations  will  be based on specific flow allowances
following subdivisions:

     1.  Scrap drying wet air pollution control,
     2.  Scrap screening and milling,
     3.  Dross washing,
     4.  Demagging wet air pollution control,
     5.  Delacquering wet air pollution control,
     6.  Ingot conveyer casting,
     7.  Direct chill casting contact cooling,
     8.  Stationary casting contact cooling, and
     9.  Shot casting contact cooling.
             for  the
                               902

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          SECONDARY ALUMINUM SUBCATEGORY
    SECT - IV
OTHER FACTORS

The other factors considered in this evaluation were shown to  be
inappropriate  bases  for further  segmentation.   Air  pollution
control  methods, treatment costs, nonwater quality aspects,  and
total energy requirements were each shown to be functions of  the
selected   subcategorization  factors  —  metal   product,   raw
materials,  and production processes.  As such, they support  the
method  of  subcategorization which has  been  applied.   Certain
other  factors, such as plant age, plant size, and the number  of
employees, were also evaluated and determined to be inappropriate
as bases for subcategorization of nonferrous metal plants.

PRODUCTION NORMALIZING PARAMETERS

The effluent limitations and standards developed in this document
establish mass limitations on the discharge of specific pollutant
parameters.   To  allow these regulations to be applied to plants
with  various  production  capacities,   the  mass  of  pollutant
discharged must be related to a unit of production.  This factor,
the production normalizing parameter (PNP), is developed for each
segment in conjunction with subcategorization.

In general,  the amount of aluminum processed or produced by  the
respective  manufacturing  process segments is used as  the  PNP.
The PNP's for the nine secondary aluminum segments are:
            Segment

1.  Scrap drying wet air pollution
    control

2.  Scrap screening and milling
3.  Dross washing

4.  Demagging wet air pollution
    control

5.  Delacquering wet air pollution
    control

6.   Ingot  conveyer casting contact
cooling

7.  Direct chill casting contact
    cooling

8.  Stationary casting contact
    cooling

9.  Shot casting contact cooling
       PNP

kkg of aluminum scrap
dried

kkg of scrap screened or
milled

kkg of dross washed

kkg of aluminum demagged
kkg of aluminum
delacquered

  kkg  of  aluminum  cast
kkg of aluminum cast
kkg of aluminum cast
kkg of aluminum cast
                               903

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SECONDARY ALUMINUM SUBCATEGORY
SECT - IV
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                    904

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           SECONDARY ALUMINUM SUBCATEGORY
SECT -V
                            SECTION V

             WATER USE AND WASTEWATER CHARACTERISTICS
This   section   describes  the  characteristics  of   wastewater
associated with the secondary aluminum subcategory.  Data used to
quantify   wastewater  flow  and  pollutant  concentrations   are
presented/   summarized,  and  discussed.   The  contribution  of
specific production processes to the overall wastewater discharge
from secondary aluminum plants is identified whenever possible.

Two  principal data sources were used in the development  of  the
effluent  limitations and standards for this  subcategory;   data
collection portfolio  (dcp) responses and field sampling results.
Data  collection portfolios, completed for each of the  secondary
aluminum plants, contained information regarding wastewater flows
and production levels.  An additional source of data used in this
document  is information and data gathered through  comments  and
Section 308 requests (used to obtain supporting documentation for
the comments).  Additional data were gathered from six plants not
considered at proposal.

Since gathering dcp information for this subcategory,  the Agency
has  learned that 15 plants have closed.   EPA believes that  the
data   from   these  plants  provide  useful  measures   of   the
relationship between production and discharge.   In light of this
conclusion,  the  Agency is using these data in its consideration
of BPT and BAT performance.

In  order  to  quantify the pollutant  discharge  from  secondary
aluminum  plants,  a  field sampling program  was  conducted.   A
complete  list of the pollutants considered and a summary of  the
techniques  used  in sampling and laboratory analyses  have  been
presented  previously.  samples  were collected  in  two  phases:
screening  and verification.  The first phase,  screen  sampling,
was  to  identify  which toxic pollutants  were  present  in  the
wastewaters  from  production of the various  metals.   Screening
samples  were  analyzed for 128 of the 129 toxic  pollutants  and
other  pollutants  deemed appropriate.  (Because  the  analytical
standard  for  TCDD  was judged to be too hazardous  to  be  made
generally  available,  samples  were  never  analyzed  for   this
pollutant.   There  is  no reason to expect that  TCDD  would  be
present in secondary aluminum wastewater.)  A total of 10  plants
were  selected  for screening sampling in the  nonferrous  metals
manufacturing  category, one of those being a secondary  aluminum
plant.

In  general,  the  samples  were analyzed for  three  classes  of
pollutants:   toxic organic pollutants,  toxic metal  pollutants,
and   criteria   pollutants  (which  includes  conventional   and
nonconventional pollutants).

As described in Section IV of this supplement, secondary aluminum
                               905

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            SECONDARY ALUMINUM SUBCATEGORY
SECT -V
 plants  have been categorized into nine  segments.    Differences  in
 the  wastewater   characteristics  associated  with   these   building
 blocks   are to be expected.   For  this reason,  wastewater   streams
 corresponding  to  each segment are  addressed  separately   in the
 discussions that follow.

 WASTEWATER SOURCES,  DISCHARGE RATES, AND  CHARACTERISTICS

 The  wastewater  data presented in this  section were evaluated   in
 light  of   production  process information compiled  during  this
 study.   As a  result,   it was possible  to identify the  principal
 wastewater  sources  in  the secondary aluminum   subcategory.   The
 result   of   this  analysis  is   summarized  in   the  following
 discussion.

 Sources of process wastewater  within  the  secondary   aluminum
 subcategory include:

      1.  Scrap drying wet air pollution control,
      2.  Scrap screening and milling,
      3.  Dross washing,
      4.  Demagging wet  air pollution control,
      5.  Delacguering wet air pollution control,
      6.  Ingot conveyer casting contact cooling,
      7.  Direct  chill casting contact cooling  water,
      8.  Stationary   casting contact cooling,  and
      9.  Shot  casting contact cooling.

 Data  supplied  by  data  collection  portfolio  responses   were
 evaluated,   and  two  flow-to-production  ratios  were  calculated for
 each  stream.   The two  ratios, water use  and wastewater discharge
 flow,   were  differentiated by the  flow  value used  in  calculation.
 Water   use   was  defined as  the volume  of water  or   other   fluid
 (e.g.,  emulsions,   lubricants)   required for  a given process per
 mass  of aluminum  product and was  therefore based on  the  sum  of
 recycle  and make-up flows to a given process.   Wastewater  flow
 discharged   after  pretreatment or  recycle (if  these are used) was
 used  in calculating  the production normalized  flow  — the  volume
 of   wastewater  discharged   from  a  given  process  to  further
 treatment,   disposal, or discharge per  mass of aluminum produced.
 Differences  between  the water  use and wastewater flows associated
 with  a  given stream resulted  from  recycle,  evaporation,  and
 carry-over on  the  product.   The production values in calculations
 correspond to  the  production  normalizing parameter, PNP, assigned
 to  each   stream,  as outlined in Section  IV.   The  production
 normalized   flows   were  compiled  by   stream    type.    Where
 appropriate,  an attempt was made to identify  factors that  could
 account  for  variations  in  water  use.    This  information  is
 summarized   in  this  section.  A  similar  analysis  of  factors
 affecting  the wastewater values is presented  in Sections X,  XI,
 and   XII,  where  representative  BAT,   BDT,  and   pretreatment
 discharge flows are selected  for use in calculating the  effluent
 limitations and standards.  As an example, casting cooling  water
wastewater  flow is related to the casting production.  As  such,
 the  discharge rate is expressed in liters of cooling  water  per
                               906

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           SECONDARY ALUMINUM SUBCATEGORY
SECT -V
metric  ton  of  casting production  (gallons  of  cooling  water
wastewater per ton of aluminum reduction production).

In  order to quantify the concentrations of pollutants present in
wastewater  from secondary aluminum  plants,  wastewater  samples
were collected at five plants.   Diagrams indicating the sampling
sites  and contributing production processes are shown in Figures
V-l to V-5 (pages 938 - 942)

The  reported  water  use  and  discharge  rates  for  the   nine
identified secondary aluminum wet operations are given in  Tables
V-l, 2, 3, 5, 7, 8, and 9 (pages 912 to 925).  The raw wastewater
sampling data for the facilities sampled are presented in  Tables
V-4T  V-6, and V-10 (pages 915, 919, and 926).  Table V-ll  (page
927) shows combined raw wastewater data from demagging  scrubbing
and casting contact cooling.

The treated wastewater data are shown in Tables V-12 through V-15
(pages  929 through 936).  The locations and stream codes of  the
samples  taken  are identified on the process  flow  diagrams  in
Figures  V-l through V-5  (pages 938 through 942).  Where no  data
is listed for a specific  day of sampling, the wastewater  samples
for  the  stream  were not collected.   If the  analysis  did  not
detect  a pollutant in a  waste stream,  the pollutant was  omitted
from the table.

The  data tables  include  some samples measured at   concentrations
considered not quantifiable.   The base neutral  extractable, acid
extractable,   and   volatile   organics   are   considered   not
quantifiable at concentrations equal to or less  than 0.010  mg/1.
Below   this  concentration,  organic analytical  results  are  not
quantitatively  accurate;  however,  the  analyses  are useful  to
indicate  the possible presence of a particular  pollutant.   The
pesticide    fraction    is  considered   not   quantifiable    at
concentrations equal to or  less than 0..005 mg/1.  Nonquantiflable
results are  designated  in the tables  with  an   asterisk   (double
asterisk  for pesticides).

These   detection  limits  shown on  the data  tables are not  the  same
as   published  detection  limits for  these pollutants by   the   same
analytical methods.  The  detection  limits  used were reported  with
the  analytical data  and  hence are the appropriate  limits  to apply
to  the data.   Detection  limit variation can occur  as a  result_of
a  number of laboratory-specific,   equipment-specific,   and daily
operator-specific factors.    These  factors  can  include  day-to-day
differences  in machine  calibration,  variation in stock  solutions,
and variation  in  operators.

The  statistical  analysis of  data includes some  samples   measured
at  concentrations considered  not  quantifiable.    Data  reported  as
 an   asterisk  are considered  as  detected but  below  quantifiable
 concentrations,  and a  value of  zero is  used for  averaging.   Toxic
 organic,  nonconventional and  conventional  pollutant data reported
 with  a  "less  than"  sign are  considered  as  detected,   but   not
 further  quantifiable.     A  value  of   zero  is  also   used   for
                                907

-------
            SECONDARY ALUMINUM SUBCATEGORY
SECT -V
 averaging.   If  a pollutant is  reported as  not   detected,   it   is
 excluded  in   calculating the   average.    Finally,   toxic   metal
 values   reported as  less than a certain value were considered   at
 not   detected,  and  a value of  zero  is  used in  the calculation  of
 the  average.    For example,  three samples  reported as  ND,  *, and
 0.021 mg/1  have an average value of  0.010 mg/1.

 In   the  following discussion,   water  use and field sampling data
 are   presented  for   each  operation.    Appropriate  tubing   or
 background   blank and source water  concentrations are  presented
 with the summaries of the sampling data.  Figures V-l through V-5
 (pages 938  through 942)  show the location of wastewater  sampling
 sites at  each facility.    The method  by which  each  sample was
 collected is  indicated by number, as  follows:

      1      one-time  grab
      2      24-hour manual  composite
      3      24-hour automatic composite
      4      48-hour manual  composite
      5      48-hour automatic composite
      6      72-hour manual  composite
      7      72-hour automatic composite

 In   the  data  collection  portfolios,  plants  were asked to specify
 the   presence  or  absence of  any  of the  toxic pollutants in   their
 effluent.   All   of  the  plants  that responded to this portion  of
 the questionnaire  indicated  that they believed the toxic  organic
pollutants  to  be  absent.   One  exception,  hexachloroethane,  was
 reported  believed  to  be  present  by two plants.   This compound was
not detected  in any  sample  taken in the subcategory.

Although  most of  the plants indicated that  the toxic metals were
believed  absent from  their effluent,   some plants did report that
specific pollutants were known present or believed present.    The
responses for  the  toxic metals are shown in the tabulation below.
Pollutant
Antimony
Arsenic
Beryllium
Cadmium
Chromium
Copper
Lead
Mercury
Nickel
Selenium
Thallium
Zinc
Known
Present
	
-
1
5
11
1
7
2
5
-
-
9
Believed
Present
_
1
—
1
5
-
6
2
2
-
-
6
Believed
Absent
23
22
22
17
7
21
10
18
16
22
22
8
Known
Absent

_
_
—
_
1
_
1
_
1
1

                               908

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           SECONDARY ALUMINUM SUBCATEGORY
SECT -V
SCRAP DRYING WET AIR POLLUTION CONTROL

Some  scrap may require drying to remove cutting oils and  water.
The  scrap  drying procedure consists of crushing the  scrap  and
heating  in  an oil or gas-fired rotary  drier.   Explosions  are
possible  in the melting furnace if the scrap is  not  completely
dried  prior to charging.   Twenty-nine secondary aluminum plants
control air emissions from scrap drying operations.  Three plants
reported the use of scrubbers,  while 26 used  baghouses.   Scrap
drying  wet  air pollution control water use and discharge  rates
are  shown  in  Table  V-l (page 912) in liters  per  metric  ton
(gal/ton)  of  aluminum scrap dried.   Plants 427 and  4102  have
either  installed  a dry system or discontinued the  use  of  the
scrubber, and plant 640 has ceased operations.

The  Agency  did  not  sample raw wastewater  from  scrap  drying
scrubbers,   however,   this  wastewater  should  contain   total
suspended solids and treatable concentrations of aluminum.  Toxic
organic   pollutants   should  not  be  present   at   measurable
concentrations.

SCRAP SCREENING AND MILLING

Only  two  plants  reported using water in  scrap  screening  and
milling.   The discharge rates from these plants are presented  in
Table  V-2 (page 913) in liters per metric ton of aluminum  scrap
screened  or milled.   The Agency did not sample scrap  screening
and milling wastewater but this waste stream should contain total
suspended  solids  and treatable concentrations of  aluminum,  as
well as toxic metals.

DROSS WASHING WASTEWATER

Sources  of aluminum for the secondary aluminum  subcategory  are
residues such as drosses,  skimmings,  and slags.  These residues
must be pretreated before charging them into the smelters.   Both
wet  and dry processes are available for this  pretreatment.   Of
the  facilities  surveyed,  four used the wet process to  prepare
their  residues for smelting.   The quantities of water used  and
discharged,  expressed  as  a function of  dross  processed,  are
presented in Table V-3 (page 914).

The  data in Table V-4 (page 915) indicate that  this  wastewater
contains  treatable concentrations of suspended solids   (aluminum
oxide  and  hydrated  alumina),   ammonia,  and  metals  such  as
aluminum, copper, and lead.

DEMAGGING WET AIR POLLUTION CONTROL

As  discussed  in Section III,  demagging consists  of  injecting
chlorine or aluminum fluoride into the molten aluminum to  remove
magnesium.  During this process, heavy fuming can result.  Of the
26 facilities supplying data,  17 reported using a wet process to
control emissions from this process,  while nine reported using a
dry  process.   The flow rates used and discharged,  expressed in
                               909

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            SECONDARY ALUMINUM SUBCATEGORY
SECT -V
 liters/metric ton of aluminum demagged,  for those plants with wet
 air pollution control are shown in Table V-5 (page 918).

 The  wastewaters  associated  with this  scrubbing  operation  may
 contain   treatable  concentrations  of   suspended   solids   and
 chlorides  or fluorides,   and of heavy metals.    Table V-6  (page
 919)  summarizes  the wastewater sampling  data  associated  with
 demagging scrubber wastes.

 DELACQUERING WET AIR POLLUTION CONTROL

 Five plants reported using  wet scrubbers to control air pollution
 from delacquering operations.   Aluminum  can scrap is charged to a
 furnace  where  paint  and   lacquers  are burned  from  the  metal
 surface.    Aluminum  fines   emitted  during  shredding  prior  to
 delacquering may also be  controlled by the  delacquering scrubber.
 Delacquering  wet air pollution control  water use  and  discharge
 rates  are shown in Table V-7  (page 923)  in liters per metric ton
 (gal/ton)  of aluminum delacquered.

 Analytical   data   supplied  to  the   Agency    show   treatable
 concentrations  of  total  phenolics  (0.346 mg/1  to  26.8   mg/1),
 suspended solids (9 mg/1  to 60.8 mg/1),  and the presence of zinc,
 lead,   and copper.   Zinc  was reported in treatable concentrations
 in   three of five samples with one  sample reported as  7.3  mg/1.
 GC/MS  data  supplied  to the   Agency show  phenol,   isophorone,
 naphthalene,   and phenanthrene at 5.4,   0.045,  0.011,   and 0.012
 mg/1,   respectively.   The   remaining toxic organics   were  all
 reported  at less than 0.010 mg/1.

 INGOT CONVEYER CASTING

 The   predominant  method  of casting  in   the secondary  aluminum
 subcategory  is   ingot conveyer  casting.  There are   17  reported
 plants  in the Agency's data base that use  contact  cooling  water
 in ingot  conveyer  casting.   There are additional  plants  that   may
 use  ingot  conveyer  casting;  however,  noncontact cooling  water   is
 used.  Water   use  and  discharge  rates obtained  from  the  dcp   are
 presented  in  Table  V-8.   Three plants reported  recycling   cooling
 water,  while  14 plants  indicated  they do   not   incorporate   any
 recycle. One plant  reported using ingot conveyer  casting   contact
 cooling water  as demagging  scrubber liquor makeup.

 Table  V-10 presents casting contact  cooling water sampling  data
 from a secondary aluminum plant  utilizing ingot conveyer casting.
 Extensive   sampling data of  direct  chill casting  is presented   in
 the aluminum forming point  source category development  document.
 These data, which are  not expected  to be significantly  different
 than  ingot conveyer casting, indicate suspended  solids, oil   and
 grease, and toxic metals may be present in both types of   cooling
waters.

DIRECT CHILL CASTING CONTACT COOLING WATER

The  Agency  is unaware of any secondary aluminum plants  in  the
                               910

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           SECONDARY ALUMINUM SUBCATEGORY
SECT -V
United  States using direct chill casting.   There are,  however,
several plants that remelt aluminum scrap for forming  operations
that use direct chill casting.  Casting of aluminum scrap for use
in  a  forming  plant is covered by the  aluminum  forming  point
source category.   Water use and discharge rates for direct chill
casting  are  presented  in  Section V of  the  primary  aluminum
subcategory supplement.

SHOT CASTING CONTACT COOLING WATER

Four   secondary  aluminum  plants  reported  casting  shot   for
subsequent  use  as a deoxidizer in the iron and steel  industry.
Water  use and discharge rates for shot casting are presented  in
Table V-9.  Temperature of the cooling water severely affects the
quality  of  the  aluminum  shot.    It  is  reported  that   the
temperature of the quench bath must be maintained between 80F and
85F in the inlet and the outlet.   Temperatures should not exceed
105F.   Two  plants  used  fresh make-up water  to  maintain  the
correct  temperature.   The other two plants,  however,  reported
using  cooling towers with no blowdown.   Pollutant  loadings  of
shot  casting  contact  cooling  water are expected  to  be  very
similar to ingot conveyer casting and direct chill casting, since
all  of  these processes use water to cool and  cast  the  molten
metal.   Oil  and  grease  should not  be  present  because  mold
lubrication is not required for shot casting.

STATIONARY CASTING COOLING

In the stationary casting method,  molten aluminum is poured into
cast  iron  molds and the generally allowed  to  air  cool.   The
Agency is aware of the use of spray quenching to quickly cool the
surface  of  the molten aluminum once it is cast into the  molds;
however,  this  water  evaporates  on  contact  with  the  molten
aluminum.   This  operation is similar throughout  the  secondary
aluminum  and  primary aluminum subcategories,  and the  aluminum
forming  category,  and  no discharge of process water  has  been
reported.
                               911

-------
       SECONDARY ALUMINUM SUBCATEGORY
                       SECT -V
                        TABLE V-l

            WATER USE AND DISCHARGE RATES FOR
         SCRAP DRYING WET AIR POLLUTION CONTROL

             (1/kkg of aluminum scrap dried)
Plant Code

 00427

 04102

 00640
Percent
Recycle

   0

 100

 100
Production
Normalized
Water Use

  1057

  5111

   567.6
  Production
  Normalized
Discharge Rate

    1057

       0

       0
                           912

-------
           SECONDARY ALUMINUM SUBCATEGORY
                       SECT -V
                            TABLE V-2

                WATER USE AND DISCHARGE RATES FOR
                   SCRAP SCREENING AND MILLING

                 (1/kkg of aluminum scrap dried)
    Plant Code

     00296

     00301*
Percent
Recycle

 100

 100
Production
Normalized
Water Use

  13827

     NR
  Production
  Normalized
Discharge Rate

    0

    0
 * — HEAVY MEDIA SEPARATION
NR — DATA NOT REPORTED
                               913

-------
           SECONDARY ALUMINUM SUBCATEGORY
                       SECT -V
                            TABLE V-3

                WATER USE AND DISCHARGE RATES FOR
                          DROSS WASHING

                     (1/kkg of dross washed)
    Plant Code

     04104

     04101

     04102

     04103
Percent
Recycle

  67

 100

 100

  67*
Production
Normalized
Water Use

  32993

  78840

  58408

     NR
  Production
  Normalized
Discharge Rate

    10868

        0

        0

        0
 * — Wastewater is all evaporated
NR — Data not reported
                                914

-------
                 SECONDARY ALUMINUM SUBCATEGORY
SECT - V
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                  917

-------
            SECONDARY ALUMINUM SUBCATEGORY
                       SECT
                             TABLE  V-5

                WATER  USE  AND  DISCHARGE  RATES  FOR
                DEMAGGING WET AIR POLLUTION  CONTROL

                   (1/kkg of  aluminum demagged)
    Plant Code

      296
    4104
      332

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    596
    547

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                               918

-------
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                                           919

-------
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-------
       SECONDARY  ALUMINUM SUBCATEGORY
                       SECT -V
                        TABLE V-7

            WATER USE AND DISCHARGE RATES FOR
         DELACQUERING WET AIR POLLUTION CONTROL

             (1/kkg of aluminum scrap dried)
Plant Code


 340

 342

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 313

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                            923

-------
        SECONDARY ALUMINUM SUBCATEGORY    SECT -V
                         TABLE V-8

             WATER USE AND DISCHARGE  RATES  FOR
          SCRAP DRYING WET AIR POLLUTION  CONTROL

              (1/kkg  of aluminum scrap dried)
Plant Code

  14
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 307
 309
 312

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                          924

-------
       SECONDARY ALUMINUM SUBCATEGORY
                       SECT -V
                        TABLE V-9

            WATER USE AND DISCHARGE RATES FOR
         SCRAP DRYING WET AIR POLLUTION CONTROL

             (1/kkg of aluminum scrap dried)
Plant Code

   51

  326

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                            925

-------
                                SECONDARY  ALUMINUM  SUBCATEGORY
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-------
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-------
                    SECONDARY ALUMINUM SUBCATEGORY
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-------
             SECONDARY ALUMINUM SUBCATEGORY
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-------
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-------
               SECONDARY ALUMINUM SUBCATEGORY
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-------
                 SECONDARY ALUMINUM  SUBCATEGORY
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-------
    SECONDARY ALUMINUM SUBCATEGORY
SECT - V
                            078  VGA BLANK
DEMAGGING
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SETTLING
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                  Figure V-l

SAMPLING SITES AT  SECONDARY ALUMINUM PLANT A
                      938

-------
  SECONDARY ALUMINUM SUBCATEGORY     SECT - V
                   066   VOA BLANK
                                  0.0140 MGD





                         RECYCLE TO BALL MILL
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                   Figure V-2



SAMPLING SITES AT SECONDARY  ALUMINUM PLANT B
                      939

-------
      SECONDARY ALUMINUM SUBCATEGORY
SECT - V
SOURCE
WATER
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                    Figure V-3
  SAMPLING  SITES AT SECONDARY ALUMINUM PLANT C
                       940

-------
      SECONDARY ALUMINUM SUBCATEGORY     SECT - V
                           097  I   VOA BLANK
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                        Figure V-4

   SAMPLING SITES AT SECONDARY ALUMINUM PLANT D
                            941

-------
       SECONDARY ALUMINUM SUBCATEGORY
                         SECT  - V
                                      SOURCE WATER
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                       Figure V-5

   SAMPLING SITES AT  SECONDARY ALUMINUM PLANT E
                          942

-------
          SECONDARY ALUMINUM SUBCATEGORY    SECT - VI







                            SECTION VI



                     SELECTION OF POLLUTANTS
This  section  examines the chemical analysis data  Ped  in
section V and discusses the selection or exclusion of



                                                  (i
or   exclude   pollutants  for  further  consideration    in    the
limitation for this subcategory.




further   considered   if   they  are   Present   in   o    .      Th
i-rpatable  bv the  technologies  considered  in  this analysis.    "»*




achievable   by carbon adsorption.







 total phenols ?by 4-AAP method) is 0.005 mg/1, which is below the
 0 010 mq/1 accepted for the other toxic organics.  However, to be





 raised treatment performance  value. No Joxic organic  pollutants
 £awa h<=Pn selected for further consideration for  limitation as  a
 rlsSlt  Sf the  revised treatment performance.   However,   sampling





                                                                i
 limitation.
                                 943

-------
            SECONDARY ALUMINUM SUBCATEGORY
SECT - VI
  CONVENTIONAL AND  NONCONVENTIONAL  POLLUTANT PARAMETERS

  This  study  examined samples from  the  secondary aluminum  subcate-
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  total suspended solids, and pH) and seven nonconventional pollu-
  tant  _parameters   (ammonia,  chemical  oxygen  demand,   chloride,
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  CONVENTIONAL AND NONCONVENTIONAL POLLUTANT PARAMETERS SELECTED

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      aluminum
      ammonia
      total phenols (4-AAP)
      total suspended solids (TSS)
      oil and grease
      pH

 Aluminum  was found above the 1.49 mg/1 concentration  attainable
 by  identified  treatment  technology in four of  six  samples  in
 three plants.    Because it is the  major product of plants in this
 subcategory and was found at  treatable  concentrations,   aluminum
 is selected for consideration for  limitation.

 Ammonia  was  measured  at three   sites   at   two  plants.     The
 concentration    of  ammonia   in these  samples   varied    widely,
 depending on the stage and type of manufacturing  process.   Those
 plants  that produce treatable  concentrations of  ammonia  will  be
 considered for  limitation  for  that pollutant.

 Total   suspended   solids   ranged from  60  to 20,140   mg/1   in  six
 samples.   All  of  the  measured  concentrations are we]1 above  the
 concentration   achievable  by   identified  treatment  technology.
 Furthermore, most  of the technologies  used to remove  toxic metals
 do _so by  converting these metals to  precipitates,  and   these
 toxic-metal-containing precipitates   should  not  be  discharged.
 Meeting a  limitation on total suspended solids also  ensures   that
 sedimentation  to   remove  precipitated  toxic  metals  has   been
 effective.    For   these   reasons,   total  suspended,  solids   is
 considered for limitation  in this subcategory.

 Data   solicited  by the Agency  through data   collection   requests
 have  demonstrated  the presence of 4-AAP phenols in  delacquering
 scrubber liquor.  Five sample analyses were submitted to EPA with
phenolics  concentrations ranging from 0.346 mg/1 to  26.8  mg/1
Three   concentrations  were  greater  than  3  mg/1.   The  toxic
pollutant phenol (number 65) was found at 5.4 mg/1 in one sample.
Based on this concentration and its frequency in delacquering wet
air  pollution  control  wastewater,  total  phenols  (4-AAP)  is
selected for consideration for limitation.
                               944

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          SECONDARY ALUMINUM SUBCATEGORY
              SECT - VI
Oil  and grease was found above its treatable  concentration  (10
mg/1) in six of seven samples with concentrations ranging from 16
to  157  mg/1.   Sampling  data  from direct  chill  casting  raw
wastewater  taken at aluminum forming plants show oil and  grease
present  at treatable concentrations in 15 of  23  samples.   The
treatable  concentrations range from 15 to 226 mg/1.   Therefore,
oil and grease is selected for consideration for limitation.

The   pH  of  a  wastewater  measures  its  relative  acidity  or
alkalinity.   In  this  study,  the  pH values  observed  in  raw
wastewater ranged from 2.8  to 9.6.   Effective removal of  toxic
metals   by   precipitation  requires  careful  control  at   pH.
Therefore, pH is considered for limitation in this subcategory.

TOXIC POLLUTANTS

The  frequency  of  occurrence of the  toxic  pollutants  in  the
wastewater  samples taken is presented in Table VI-1 (page  953).
These  data provide the basis for the categorization of  specific
pollutants,  as discussed below.  Table VI-1 is based on the  raw
wastewater  data from streams 3, 68, 70, 80, and 84 (see  Section
V).   Treatment  plant sampling data were not considered  in  the
frequency count.

TOXIC POLLUTANTS NEVER DETECTED

The  toxic  pollutants listed in Table VI-2 (page 957)  were  not
detected  in  any  wastewater  samples  from  this   subcategory;
therefore,   they   were  not  selected  for   consideration   in
establishing limitations.
TOXIC    POLLUTANTS   NEVER
QUANTIFICATION LIMIT
FOUND
ABOVE
THEIR
ANALYTICAL
The  toxic pollutants listed below were never found  above  their
analytical  quantification level in any wastewater  samples  from
this   subcategory;  therefore,  they  were  not   selected   for
consideration in establishing limitations.

      91.  chlordane
      92.  4,4'-DDT
      93.  4,4'-DDE
      98.  endrin
      99.  endrin aldehyde
     100.  heptachlor
     101.  heptachlor epoxide
     102.  alpha-BHC
     103.  beta-BHC
     104.  gamma-BHC
     106.  PCB-1242      (a)
     107.  PBC-1254      (a)
     108.  PCB-1221      (a)
     109.  PCB-1232      (b)
     110.  PCB-1248      (b)
     111.  PCB-1260      (b)
                               945

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           SECONDARY  ALUMINUM SUBCATEGORY
                   SECT - VI
      112.   PCB-1016
      113.   toxaphene
      121.   cyanide
(b)
      (a),(b)  Reported  together.

TOXIC POLLUTANTS   PRESENT   BELOW
TREATMENT
          CONCENTRATIONS   ACHIEVABLE   BY
The  pollutants  listed below were  not  selected  for  consideration
in  establishing limitations because they were  not found  in  any
wastewater  samples   from  this  subcategory  above  concentrations
considered   achievable  by  existing  or   available   treatment
technologies.     These   pollutants  are  discussed  individually
following the list.

     114.  antimony
     117.  beryllium
     123.  mercury
     125.  selenium
     126.  silver

Antimony  was found above  its analytical quantification limit  in
one of six samples collected at four plants.    The  concentration
found  was  0.3  mg/1,   which   was   below  that  achievable  by
identified  technology.    Therefore,   antimony  was not considered
for limitation.

Beryllium  was found  above its analytical quantification limit in
three  of four samples.    The maximum  concentration measured  was
0.20 mg/1.   The concentration achievable by identified treatment
technology  are  0.20  mg/1.    Therefore,   beryllium   was  not
considered for limitation.

Mercury was detected  above its analytical quantification limit in
all  five  samples of this subcategory,  ranging from  0.0002  to
0.0064  mg/1.   All   of  the values were  below the  0.036  mg/1
concentration  achievable  by  identified  treatment  technology.
Therefore, mercury was not considered  for limitation.

Selenium  was found above  its quantification concentration in one
of  three samples collected at three plants.    The  concentration
found  was 0.20 mg/1,  which was. the concentration achievable  by
identified  treatment technology.   Therefore,  selenium was  not
considered for limitation.

Silver was found above its analytical quantification limit in one
of three samples with a value of 0.07 mg/1.   This  concentration
was  equal to that achievable by identified treatment technology.
Therefore, silver  are not considered for limitation.

TOXIC POLLUTANTS DETECTED  IN A SMALL NUMBER OF  SOURCES

The  following pollutants  were not selected for consideration for
limitation on the basis they were detectable in the effluent from
                               946

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          SECONDARY ALUMINUM SUBCATEGORY
SECT - VI
only  a small number of sources within the subcategory and it  is
uniquely related to only those sources.

       4.  benzene
      23.  chloroform
      27.  1,4-dichlorobenzene
      29.  1,1-dichloroethylene
      30.  1,2-trans-dichloroethylene
      39.  fluoranthene
      44.  methylene chloride
      48.  dichlorobromomethane
      66.  bis(2-ethylhexyl) phthalate
      67.  butyl benzyl phthalate
      68.  di-n-butyl phthalate
      69.  di-n-octyl phthalate
      71.  dimethyl phthalate
      73.  benzo(a)pyrene
      76.  chrysene
      77.  acenaphthylene
      84.  pyrene
      85.  tetrachloroethylene
      87.  trichloroethylene
     115.  arsenic
     119.  chromium
     120.  copper
     124.  nickel
     127.  thallium

Although  these pollutants were not selected for consideration in
establishing nationwide limitations,  it may be appropriate, on a
case-by-case  basis,  for the permit writer to  specify  effluent
limitations.

Benzene  was found above its analytical quantification  limit  in
one of 12 samples collected at four plants.  The concentration of
0.136  mg/1 was above the concentration achievable by  identified
treatment  technology.    Also,  all  secondary  aluminum  plants
indicated  in the. dcp that this pollutant was known to be  absent
or  believed to be absent from their wastewater.   Because it was
found above a treatable concentration at only one plant,  benzene
was not considered for limitation.

Chloroform,  a  common laboratory solvent,  was found  above  its
analytical  quantification limit in 10 of 12 samples collected at
four plants.  The 10 samples ranged from values of 0.019 to 0.410
mg/1  which  were  at concentrations  above  that  achievable  by.
treatment.    All  secondary aluminum-plants indicated in the  dcp
that  this  pollutant  was known to be absent or believed  to  be
absent from their wastewater.   Because the possibility of sample
contamination  is  likely,  chloroform  was  not  considered  for
limitation.

1,4-Dichlorobenzene was found above its analytical quantification
concentration  in  only one of six samples collected  from  three
plants with a concentration of 0.026 ing/1, which was treatable by
                               947

-------
          SECONDARY ALUMINUM SUBCATEGORY
SECT - VI
identified technology.   However,  all secondary aluminum  plants
indicated  in the dcp that this pollutant was known to be  absent
or  believed  to be absent from their wastewater.   Since it  was
detected   in  only  one  plant,   1,4-dichlorobenzene  was   not
considered for limitation.

1,1-Dichloroethylene  was  detected  in only one  of  12  samples
collected  at  four plants.   Its concentration was  0.099  mg/1,
which  was  above  the  concentration  achievable  by   available
treatment (0.010 mg/1).   Because it was found at only one plant,
indicating  the pollutant is site-specific,  1,1-dichloroethylene
was not considered for limitation.

1,2-trans-Dichloroethylene   was   found  above   its   treatable
concentration  (0.010  mg/1) in five of  12  samples.   All  five
samples  were  taken  at the same  plant,  including  three  from
demagging scrubber wastewater.   However,  this pollutant was not
detected  in six samples from three other plants.   Five of these
six  samples  were taken from demagging  scrubber  wastewater  or
combined  wastewater  including  demagging  scrubber  wastewater.
Also,   all  secondary  aluminum  plants  reporting  in  the  dcp
indicated  that  this pollutant was believed to  be  absent  from
their  wastewater.   Since this pollutant was found in  treatable
concentrations at only one plant, indicating it is site-specific,
1,2-trans-dichloroethylene was not considered for limitation.

Pluoranthene  was  detected above its  analytical  quantification
limit in only one of six samples collected at three plants.   The
reported  fluoranthene concentration,  0.020 mg/1,  was above the
concentration achievable by available  treatment.   However,  all
secondary   aluminum  plants  indicated  in  the  dcp  that  this
pollutant  was known to be absent or believed to be  absent  from
their  wastewater.   Because  it  was found at.  only  one  plant,
indicating  the pollutant is site-specific,  fluoranthene was not
considered for limitation.

Methylene chloride was found above its analytical  quantification
limit  in  one of 12 samples.   The measurable concentration  was
0.370  mg/1.   This  pollutant was not attributable  to  specific
materials  or  processes associated with the  secondary  aluminum
subcategory;  however,  it is a common solvent used in analytical
laboratories.   Also,  all secondary aluminum plants indicated in
the dcp that this pollutant was known to be absent or believed to
be absent from their•wastewater.  Since the possibility of sample
contamination  was likely,  methylene chloride is not  considered
for limitation.

Dichlorobromomethane  was  detected  in only one  of  12  samples
collected  at  four plants.   Its concentration was  0.019  mg/1,
which  was  above  the  concentration  achievable  by   available
treatment (0.010 mg/1).   Because it was found at only one plant,
indicating the pollutant was site-specific,  dichlorobromomethane
was not considered for limitation.

Bis(2-ethylhexyl)   phthalate  was  found  above  its  analytical
                               948

-------
          SECONDARY ALUMINUM SUBCATEGORY
SECT - VI
quantification limit in three of six samples.  The concentrations
measured were 0.075,  0.28f  and 2.03 rag/1.  The presence of this
pollutant   was  not  attributable  to  materials  or   processes
associated  with  the  secondary  aluminum  subcategory.   It  is
commonly  used as a plasticizer in laboratory and field  sampling
equipment.  EPA  suspects sample contamination as the  source  of
this  pollutant.   Also,  all secondary aluminum plants indicated
in the dcp that this pollutant was known to be absent or believed
to be absent from their wastewater.  Therefore, bis(2-ethylhexyl)
phthalate was not considered for limitation.

Butyl   benzyl   phthalate   was  found  above   its   analytical
quantification  limit in two of six samples collected from  three
plants.  The  measured  values were 0.014 and  0.098  mg/1.   The
presence  of this pollutant was not attributable to materials  or
processes associated with the secondary aluminum subcategory.  It
is  commonly  used  as  a plasticizer  in  laboratory  and  field
sampling  equipment.   EPA suspects sample contamination  as  the
source  of this pollutant.   Also,  all secondary aluminum plants
indicated  in the dcp that this pollutant was known to be  absent
or  believed  to  be absent from  their  wastewater.   For  these
reasons,   butyl   benzyl  phthalate  was  not   considered   for
limitation.

Di-n-butyl    phthalate   was   found   above   its    analytical
quantification  limit in two of six samples,  with concentrations
of 0.022 and 0.045 mg/1.   The presence of this pollutant was not
attributable  to  materials  or  processes  associated  with  the
secondary  aluminum  subcategory.   It  is  commonly  used  as  a
plasticizer  in  laboratory and field  sampling  equipment.   EPA
suspects  sample  contamination as the source of this  pollutant.
Also,  all  secondary aluminum plants indicated in the  dcp  that
this  pollutant  was known to be absent or believed to be  absent
from their wastewater.   Therefore,  di-n-butyl phthalate was not
considered for limitation.

.Di-n-octyl    phthalate   was   found   above   its    analytical
quantification  limit  in only one of six  samples  collected  at
three plants,  at a concentration of 0.036 mg/1.  The presence of
this  pollutant  was not attributable to materials  or  processes
associated  with  the  secondary  aluminum  subcategory.   It  is
commonly  used as a plasticizer in laboratory and field  sampling
equipment.   EPA  suspects sample contamination as the source  of
this pollutant.  Also, all secondary aluminum plants indicated in
the dcp that this pollutant was known to be absent or believed to
be absent from their wastewater.   For these reasons,  di-n-octyl
phthalate was not considered for limitation.

Dimethyl  phthalate was detected at a concentration greater  than
its  analytical  quantification limit in only one of six  samples
collected  at three plants.   The measured concentration of  this
toxic  pollutant was 0.056 mg/1.   Also,  all secondary  aluminum
plants  indicated in the dcp that this pollutant was known to  be
absent or believed to be absent from their  wastewater.   Because
it  was  found  at  just one plant,  dimethyl  phthalate  was not
                               949

-------
          SECONDARY ALUMINUM SUBCATEGORY
SECT - VI
considered for limitation.

Benzo(a)pyrene   was  detected  at  a  concentration  above   its
analytical  quantification  limit  in  only one  of  six  samples
collected at three plants.  The 0.012 mg/1 concentration measured
was  above the concentration achievable by  identified  treatment
technology.  However,  all secondary aluminum plants indicated in
the dcp that this pollutant was known to be absent or believed to
be  absent from their wastewater.   Because it was found at  only
one plant, benzo(a)pyrene was not considered for limitation.

Chrysene  was  detected at a concentration above  its  analytical
quantification  limit  in  only one of six samples  collected  at
three  plants.   The 0.017 mg/1 concentration measured was  above
the concentration achievable by identified treatment  technology.
However,  all secondary aluminum plants indicated in the dcp that
this  pollutant  was known to be absent or believed to be  absent
from their wastewater.   Because it was found only at one  plant,
chrysene was not considered for limitation.

Acenaphthylene   was  detected  at  a  concentration  above   its
analytical  quantification  limit  in  only one  of  six  samples
collected at three plants.  The 0.017 mg/1 concentration measured
was  above the concentration achievable by  identified  treatment
technology.  Also, all secondary aluminum plants indicated in the
dcp  that this pollutant was known to be absent or believed to be
absent from their wastewater.   Because it was found at only  one
plant, acenaphthylene was not considered for limitation.

Pyrene   was  measured  at  a  concentration  greater  than   its
analytical  quantification  limit  in  only one  of  six  samples
collected  at  three plants.   The concentration  of  this  toxic
pollutant  was 0.024 mg/1.   Also,  all secondary aluminum plants
indicated  in the dcp that this pollutant was known to be  absent
or believed to be absent from their wastewater.   Because it  was
found   at  just  one  plant,   pyrene  was  not  considered  for
limitation.

Tetrachloroethylene was found above its analytical quantification
limit  and  above  the  concentration  attainable  by   available
treatment  in only one of 12 samples collected from four  plants,
indicating  the  pollutant  was  site-specific.    The   measured
concentration  was  0.378 mg/1.   Also,  all  secondary  aluminum
plants  indicated in the dcp that this pollutant was known to  be
absent   or   believed  to  be  absent  from  their   wastewater.
Therefore, tetrachloroethylene was not considered for limitation.

Trichloroethylene  was found above its analytical  quantification
limit and treatable concentration in one of 12 samples  collected
from four plants.  The sample concentration was 0.787 mg/1. Also,
all  secondary  aluminum  plants indicated in the dcp  that  this
pollutant  was known to be absent or believed to be  absent  from
their  wastewater.   Since  this pollutant was found at only  one
plant, trichloroethylene was not considered for limitation.
                               950

-------
          SECONDARY ALUMINUM SUBCATEGORY
SECT - VI
Arsenic  was  found above its treatable concentration in  one  of
three  samples collected at four plants.   The  concentration  of
arsenic  was  4.0  mg/1.  Since  it  was  found  at  a  treatable
concentration  only  one plant,  arsenic was not  considered  for
limitation.

Chromium  was found above its treatable concentration in  one  of
three samples collected at two plants.  This sample contained 2.0
mg/1  of chromium.   Since a treatable concentration of  chromium
was collected at only one plant,  chromium was not considered for
limitation.

Copper was found above its treatable concentration in one of four
samples,  with a value of 10.0 mg/1.   Since copper was found  at
only  one plant,  it was considered specific to that site and was
not considered for limitation.

Nickel  was detected above its treatable concentration in one  of
three samples (1.0 mg/1).   Since it was found in only one plant,
nickel was not considered for limitation.

Thallium was detected above its treatable concentration in one of
three samples collected at three plants.  Because it was found at
only one plant,  thallium was not considered for limitation.

TOXIC  POLLUTANTS  SELECTED  FOR CONSIDERATION  FOR  ESTABLISHING
LIMITATIONS

The   pollutants  listed  below  were   selected    for   further
consideration   in establishing  limitations and standards for this
subcategory.    The toxic pollutants selected are  each  discussed
following  the list.

       65.  phenol
      118.  cadmium
      122.   lead
      128.   zinc

Phenol   was   detected   in  one  of  three   samples  above  treatable
concentrations.    Delacquering  wet    air    pollution   control
wastewater,   based   on   data   from  one  sample   submitted  to  the
Agency,   contains phenol.   Also,  the  data  show  that delacquering
wet   air pollution control wastewater  contains total phenolics in
concentrations   up to  26.8 mg/1.    In five  analyses  submitted   to
the  Agency,  total phenolics  was above treatable  concentrations in
all    five   samples.    Therefore,    phenol   was    selected   for
consideration for  limitation.

Cadmium was detected above its analytical  quantification  limit in
 four  samples collected at two plants.   The  values   ranged  from
 0.020 to 0.500  mg/1.   Three of the concentrations were above  the
 concentration   of   0.049   mg/1,    which  is   achievable   by  the
 identified  treatment  technology.    Data  supplied to EPA  by   an
 industry representative showed cadmium at  0.64 mg/1  in one  sample
 from delacquering wet air  pollution control.    Therefore,  cadmium
                                951

-------
          SECONDARY ALUMINUM SUBCATEGORY
SECT - VI
was selected for consideration for limitation.

Lead  was  detected present above its  analytical  quantification
limit in all four samples collected at two plants.   The reported
lead  concentrations  ranged  from 0.060 to  8.0  mg/1.   A  lead
concentration of 0.08 mg/1 is achievable by identified  treatment
technology.   Data  supplied  to EPA by industry  representatives
showed lead above treatable concentrations in two of five samples
(0.1  and 2.1 mg/1) for delacquering wet air  pollution  control.
Therefore, lead was selected for consideration for limitation.

Zinc  was  detected above its analytical quantification limit  in
all four samples collected at two plants.   The concentrations of
zinc reported ranged from 2.0 to 8.0 mg/1.   The concentration of
zinc achievable by identified treatment technology is 0.23  mg/1.
Data  supplied  to  EPA by industry representatives  showed  zinc
above  treatable concentrations in three of five samples  (0.824,
0.898,  and 7.3 mg/1) for delacquering wet air pollution control.
Therefore, zinc was selected for consideration for limitation.
                               952

-------
                   SECONDARY ALUMINUM SUBCATEGORY
                                                              SECT  - VI
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-------
   SECONDARY ALUMINUM SUBCATEGORY
SECT - VI
                    TABLE VI-2

           TOXIC POLLUTANTS NEVER DETECTED

 1.   acenaphthene
 2.   acrolein
 3.   acrylonitrile
 5.   benzidine
 6.   carbon tetrachloride
 7.   chlorobenzene
 8.   1,2,4-trichlorobenzene
 9.   hexachlorobenzene
10.   1,2-dichloroethane
11.   1,1,1-trichloroethane
12.   hexachloroethane
13.   ifl-dichloroethane
14.   1,1,2-trichloroethane
15.   1,1,2,2-tetrachloroethane
16.   chloroethane
17.   DELETED
18.   bis(2-chloroethyl) ether
19.   2-chloroethyl vinyl ether
20.   2-chloronaphthalene
21.   2,4,6-trichlorophenol
22.   parachlorometa cresol
24.  2-chlorophenol
25.  1,2-dichlorobenzene
26.  1,3-dichlorobenzene
28.  3,3'-dichlorobenzidine
31.  2,4-dichlorophenol
32.  If2-dichloropropane
33.  1,3-dichloropropylene
34.  2,4-dimethylphenol
 35.  2,4-dinitrotoluene
 36.  2,6-dinitrotoluene
 37.  lf2-diphenylhydrazine
 38.  ethylbenzene
 40.  4-chlorophenyl  phenyl  ether
 41.  4-bromophenyl phenyl ether
 42.  bis(2-chloroisopropyl)  ether
 43.  bis(2-chloroethoxy)  methane
 45.  methyl chloride
 46.  methyl bromide
 47.   bromoform
 49.   DELETED
 50.   DELETED
 51.   chlorodibromomethane
 52.   hexachlorobutadiene
 53.   hexachlorocyclopentadiene
 54.   isophorone
 55.   naphthalene
 56.   nitrobenzene
 57.   2-nitrophenol
                          957

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      SECONDARY ALUMINUM SUBCATEGORY
                                  SECT - VI
  58.
  59.
  60.
  61.
  62.
  63.
  64.
  70.
  72.
  74.
  75.
  78.
  79.
  80.
  81.
  82.
  83.
  86.
  88.
  89.
  90.
  94.
  95.
  96.
  97.
105.
116.
129.
           TABLE VI-2 (Continued)

       TOXIC POLLUTANTS NEVER DETECTED


 4-nitrophenol
 2,4-dinitrophenol
 4,6-dinitro-o-cresol
 N-nitrosodimethylamine
 N-nitrosodiphenylamine
 N-nitrosodi-n-propylamine
 pentachlorophenol
 diethyl  phthalate
 benzo(
 3,4-be
 benzo(
 anthra
 benzo(gh
       )anthracene
    benzofluoranthene
    o(k)fluoranthene
anthracene (a)
fluorene
         . Jperylene
phenanthrene  (a)
dibenzo(a,h)anthracene
indeno  (1,2,3-cd)pyrene
toluene
vinyl chloride
aldrin
dieldrin
4,4'-ODD
alpha-endosulfan
beta-endosulfan
endosulfan sulfate
delta-BHC
asbestos
2,3,7,8-tetrachlorodibenzo-p-dioxin (TCDD)
 (a)   Reported together
                         958

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         SECONDARY ALUMINUM SUBCATEGORY    SECT - VII



                            SECTION VII

                CONTROL AND TREATMENT TECHNOLOGIES


The   preceding   sections  of  this  supplement  discussed   the
wastewater sources, flows, and characteristics of the wastewaters
from  secondary  aluminum plants.   This section  summarizes  the
description  of  these  wastewaters and indicates  the  level  of
treatment  which is currently practiced by in secondary  aluminum
subcategory for each waste stream.   Since gathering data through
data collection portfolios, the Agency has learned that 15 plants
have  closed.   Treatment methods used by these plants are  still
presented  in this section because they play an integral part  in
BAT technology selection.

This  section  presents a summary of the  control  and  treatment
technologies  that  are currently being applied to  each  of  the
sources generating wastewater in this subcategory.  As  discussed
in  Section V, wastewater associated with the secondary  aluminum
subcategory  is characterized by the presence of the toxic  metal
pollutants and suspended solids.  The raw (untreated)  wastewater
data are presented for specific sources as well as combined waste
streams in Section V.  Generally, these pollutants are present in
each  of the waste streams at treatable concentrations, so  these
waste  streams are commonly combined for treatment to reduce  the
concentrations   of  these  pollutants.   Construction   of   one
wastewater treatment system for combined treatment allows  plants
to  take advantage of economies of scale and, in some  instances,
to  combine streams of differing alkalinity to  reduce  treatment
chemical   requirements.   Three  plants  in   this   subcategory
currently  have  combined wastewater treatment systems,  one  has
lime  precipitation  and sedimentation, and no plants  have  lime
precipitation,  sedimentation  and  filtration.   As  such,   two
options  have been selected for consideration for BAT,  BDT,  and
pretreatment in this subcategory, based on combined treatment  of
these compatible waste streams.

TECHNICAL BASIS OP EXISTING REGULATIONS

As  mentioned  in  Section  III,  EPA  promulgated ^BPT  effluent
limitations   guidelines  for  the  secondary  aluminum  smelting
subcategory  on April 8,  1974.   In order to put  the  treatment
practices  currently  in place and the technologies selected  for
BAT  options  into the proper perspective,  it  is  necessary  to
describe  the  technologies selected by EPA  for  BPT,  BAT,  and
pretreatment  standards.   The BPT regulations established by EPA
limited  the discharge of  aluminum,   copper,  ammonia,  chemical
oxygen demand,  fluoride, and total suspended solids and required
the  control  of pH  (refer to Section  IX).   The  BAT  regulation
required  zero  discharge  based  on   in-process  changes   which
eliminated   the need for demagging wet air pollution control  and
dross  washing.    Zero discharge  of metal cooling water was based
on  100  percent   recycle.   Pretreatment  for  existing  sources


                                959

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         SECONDARY ALUMINUM SUBCATEGORY
SECT
VII
required oil skimming, pH adjustment, and ammonia air stripping.

SCRAP DRYING WET AIR POLLUTION CONTROL

Wet  and  dry control devices are used to control  air  emissions
from  scrap drying operations.   Three plants use  scrubbers;  26
plants use baghouses.   Two plants practice 100 percent  recycle,
resulting   in  zero  discharge.    One  plant  discharges   this
wastewater, which may contain suspended solids and aluminum.

Alkali addition and sedimentation can be used to remove suspended
solids and some metals.   The one plant producing this wastewater
reported  no  treatment before discharging to a  municipal  sewer
system.

SCRAP SCREENING AND MILLING WASTEWATER

Two plants operate scrap screening and milling operations.   Both
plants practice 100 percent reycle of this wastewater,  which may
contain  total suspended solids,  toxic metals,  and aluminum  at
treatable concentrations.   Alkali addition and sedimentation may
be used to reduce suspended solids and some metals.

DROSS WASHING WASTEWATER

Of  the  four  plants that practice  wet  dross  processing,  two
practice  100  percent recycle and one attains zero discharge  by
solar  evaporation.   Two  plants  recycle  67  percent  of  this
wastewater,  which contains toxic metals,  aluminum, ammonia, and
suspended solids.

The  only  currently  practiced  reduction  of  primary  aluminum
residues * and  secondary aluminum slags uses wet milling  with  a
countercurrent flow process to reduce or possibly eliminate  salt
impregnation  of  runoff  and ground water from  discarded  solid
waste.  Such salt recovery installations are operating in England
and Switzerland, and the salts recovered assist in pciying for the
operation  since  they  are  reusable as  fluxing  salts  in  the
secondary  aluminum  subcategory.    By  using  a  countercurrent
milling and washing approach,  two advantages are realized.   The
final  recovered metal is washed with clean  water,  providing  a
low-salt feed to the melting furnaces.   The wastewater, with the
insolubles  removed,  would  be of a concentration  suitable  for
economical  salt  recovery  by evaporation  and  crystallization.
Heat for evaporation could be supplied by the waste heat from the
furnaces.   The  process would have to contend with the  ultimate
disposal of dirt,  trace metals,  and insoluble salts not removed
from the dross during milling.  Sedimentation with recycle is the
treatment method currently used at the one discharging facility.

DEMAGGING WET AIR POLLUTION CONTROL

During  the  smelting  process it is often  necessary  to  remove
magnesium  from the molten aluminum.   This process of  demagging
can  be  performed  with chlorine  or  aluminum  fluoride.   Most
                               960

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         SECONDARY ALUMINUM SUBCATEGORY
SECT - VII
facilities  (25 of the 37 that demag)  use chlorine to  accomplish
the demagging.  Aluminum fluoride is more expensive than^chlorine
and  is  not regarded as effective  in  removing  magnesium.    In
addition,  the  furnace  refractory lining life is  shorter  when
aluminum  fluoride is used since residues resulting from its  use
in  the  demagging  process  are  more  corrosive  than  chlorine
generated residues.

However,  demagging  with chlorine complicates emissions  control
because  of  the formation of hydrochloric acid in  the  smelting
emissions,  due  to  the  hydrolysis of  aluminum  and  magnesium
chloride  when  wet scrubbing is used.   Emissions from  aluminum
fluoride demagging are usually controlled with dry processes.
Demagging scrubbing wastewater contains toxic
total suspended solids, and oil and grease.
    metals,  aluminum,
Of  the 58 facilities surveyed,  20 use some form of wet  process
control of demagging air emissions.   Four of the 20 practice 100
percent  recycle.   Four  of  the  facilities  discharge  (either
directly or to a POTW) with no prior treatment,  and one facility
only  settles  the waste stream before discharging it.   The  six
facilities that treat this waste stream all neutralize the stream
(often with soda ash) before discharge.  This neutralization step
is  usually followed by a settling procedure since pH  adjustment
to  5.0  to  7.0  will  precipitate  most  of  the  aluminum  and
magnesium.

DELACQUERING WET AIR POLLUTION CONTROL

Wet scrubbers are used to control air pollution from delacquering
operations   at   five   plants.    Two   plants   report   using
sedimentation,  one plant neutralizes with caustic, and one plant
uses  lime and settle treatment.   The fifth plant did not report
its treatment method.   Three plants reported recycle rates of  97
percent and above.

Analytical data submitted to the Agency show delacquering wet air
pollution  control  wastewater  to contain  total  phenolics  and
treatable concentrations of zinc.   The pH of the scrubber liquor
is  approximately 6.5 and TSS concentrations are typically  below
70 mg/1.

INGOT CONVEYER CASTING CONTACT COOLING

Ingot molds traveling on conveyers are sprayed with water to cool
and solidify  the molten metal.

Oil  and  grease,   used•to  lubricate mold  conveyer   systems,   is
washed   from  the equipment  as  the  product  is sprayed  with  water.
The  quantity  of   ingot conveyer  wastewater can  be   reduced  _by
recycle  or  the reuse  of the water  in demagging wet air  pollution
control.

Casting   contact cooling water contains  treatable  concentrations
                                961

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          SECONDARY ALUMINUM SUBCATEGORY
SECT - VII
 of aluminum, oil and grease, and suspended solids.

 Of  the 17 facilities known to have ingot conveyer casting,  only
 one  plant  uses  any  sort  of  treatment  prior  to  discharge.
 Wastewater treatment at this plant consists of flotation and grit
 removal.  Recycle is practiced at three plants.

 SHOT CASTING CONTACT COOLING

 The  manufacture  of  deoxidizer shot  involves  allowing  molten
 aluminum  to  flow  through  a mesh screen and  fall  (forming  a
 spherical  shot product) into a quenching tank.   There are  four
 plants known to manufacture shot,  two of them are zero discharge
 through holding tanks and cooling towers.   Chemical treatment of
 the wastewater is not practiced at any of the four plants.

 CONTROL AND TREATMENT OPTIONS CONSIDERED

 Based  on  an examination of the wastewater  sampling  data,   two
 treatment  technologies that effectively control  the  pollutants
 found  in  secondary  aluminum  wastewaters  were  selected   for
 evaluation.   These technology options are discussed below.

 OPTION A

 Option  A for the secondary aluminum subcategory is analogous   to
 BPT  treatment  with  a few  modifications.    Option  A  requires
 control  and   treatment technologies to reduce the  discharge   of
 wastewater volume and pollutant mass.   Recycle of casting contact
 cooling water is the control mechanism for flow reduction.

 The_ Option   A  treatment   model   consists   of  ammonia    stream
 stripping  pretreatment applied to the dross washing  wastewater
 stream,    activated   carbon  adsorption  pretreatment  for  total
 phenolics,    pretreatment   of   casting  cooling  water  with   oil
 skimming,  and  lime  and settle  technology (chemical precipitation
 and_ sedimentation)   applied to the   combined  stream  of  steam
 stripper effluent,   demagging air pollution scrubbing wastewater,
 delacquering  air  pollution scrubbing  wastewater,   and  casting
 contact  cooling wastewater.    Chemical precipitation is  used   to
 remove  metals   by   the  addition of   lime followed  by  gravity
 sedimentation:   Suspended   solids  are  also   removed  from   the
 process.   Option  A varies slightly  from the   promulgated   BPT
 technology  in   that  the existing BPT  requires  zero discharge   of
 metal cooling water.   Data  submitted  to  the Agency (see  Section
 IX) have demonstrated the need  for a blowdown  from  ingot  conveyer
 casting  when demagging scrubbers are  not  operated.   Therefore,
 Option  A  includes   90 percent  recycle  of  cooling  water  when
 demagging  wet   air pollution control  is not practiced,   and   100
 percent  reuse   when  demagging  wet   air  pollution  control   is
 practiced.

OPTION C

Option  C  for   the secondary aluminum  subcategory  consists  of
                               962

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         SECONDARY ALUMINUM SUBCATEGORY
SECT - VII
preliminary treatment with ammonia steam stripping, oil skimming,
activated carbon adsorption,  in-process flow reduction,  and the
chemical precipitation and sedimentation technology considered in
Option  A  plus  multimedia  filtration  end-of-pipe  technology.
Multimedia   filtration  is  used  to  remove  suspended  solids,
including  precipitates  of  metals,   beyond  the  concentration
attainable by gravity sedimentation.   The filter suggested is of
the  mixed media type,  although other forms of filters  such  as
rapid   sand   filters   or  pressure   filters   would   perform
satisfactorily.  The addition of filters also provides consistent
removal  during  periods  in which there are rapid  increases  in
flows or loadings of pollutants to the treatment scheme.

CONTROL AND TREATMENT OPTIONS REJECTED

Prior  to proposing mass limitations for the  secondary  aluminum
subcategory,  the  Agency evaluated reverse osmosis as an end-of-
pipe treatment technology.  However, reverse osmosis was rejected
because   it  is  not  demonstrated  in  the  nonferrous   metals
manufacturing subcategory,  nor is it clearly transferable.   The
Option F treatment scheme is discussed below.

Option  F  for the secondary aluminum  subcategory  consisted  of
preliminary  treatment  with  ammonia  steam  stripping  and  oil
skimming  in-process  flow  reduction,   chemical  precipitation,
sedimentation, and multimedia filtration technology considered in
Option  C  with the addition of reverse osmosis  and  evaporation
end-of-pipe technology.  Option F is used for complete recycle of
the  treated water by controlling the concentration of  dissolved
solids. Multiple-effect evaporation is used to dewater the brines
rejected from reverse osmosis.
                               963

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SECONDARY ALUMINUM SUBCATEGORY
SECT - VII
      THIS  PAGE  INTENTIONALLY  LEFT  BLANK
                     964

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         SECONDARY ALUMINUM SUBCATEGORY
SECT - VIII
                           SECTION VIII

           COSTS, ENERGY, AND NONWATER QUALITY ASPECTS
This  section  describes  the method used to  develop  the  costs
associated with the control and treatment technologies  discussed
in  Section  VII for wastewaters from secondary aluminum  plants.
The  energy requirements of the considered options,  as  well  as
solid waste and air pollution aspects, are also discussed in this
section.

TREATMENT OPTIONS CONSIDERED

As  discussed in Section VII,  two control and treatment  options
are   considered  for  treating  wastewater  from  the  secondary
aluminum subcategory.  Cost estimates, in the form of annual cost
curves,  have  been  developed  for each  of  these  control  and
treatment   options.  The  control  and  treatment  options   are
presented  schematically  in Figures X-l and X-2 (pages  995  and
996) and summarized below.

OPTION A

Option  A for the secondary aluminum subcategory requires control
and treatment technologies to reduce the discharge of  wastewater
volume and pollutant mass.  The recycle of ingot conveyer casting
contact cooling water through cooling towers or 100 percent reuse
in  demagging  scrubbers  and the recycle  of  scrap  drying  and
delacquering scrubber water through holding tanks are the control
mechanisms for flow reduction.  The Option A treatment technology
consists of ammonia steam stripping preliminary treatment applied
to  the  dross  washing  wastewater  stream,  and  oil   skimming
preliminary  treatment  applied to the  casting  contact  cooling
water stream.  Activated carbon adsorption preliminary  treatment
is  required  for  phenolics  in  delacquering  scrubber  liquor.
Preliminary  treatment  is  followed by  lime  precipitation  and
sedimentation  applied to the combined stream of  steam  stripper
effluent,  casting contact cooling water,  delacquering  scrubber
blowdown, and demagging scrubber water.

OPTION C

Option  C for the secondary aluminum subcategory consists of  all
the  control  and treatment technologies of Option A   (in-process
flow reduction through holding tanks and cooling towers,  ammonia
steam stripping and oil skimming preliminary treatment,  and lime
precipitation  and sedimentation end-of-pipe treatment) with  the
addition  of multimedia filtration to the  end-of-pipe  treatment
scheme.
                               965

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          SECONDARY ALUMINUM SUBCATEGORY
SECT - VIII
 Cost Methodology

 A  detailed  discussion  of the methodology used to  develop  the
 compliance  costs  is presented in Section VIII  of  the  General
 Development Document.   Plant-by-plant compliance costs have been
 estimated   for  the  secondary  aluminum  subcategory  and   are
 presented   in   the   administrative  record   supporting   this
 regulation.  A comparison of the costs, developed for proposal and
 the  revised  costs  for the final regulation  are  presented  in
 Tables  VIII-1 and VIII-2 (pages 970 and 971) for the direct  and
 indirect dischargers, respectively.

 Each of the major assumptions used to develop compliance costs is
 presented  in  Section VIII of the General Development  Document.
 Each subcategory contains a unique set of waste streams requiring
 certain  subcategory-specific assumptions to  develop  compliance
 costs.  Seven major assumptions are  discussed briefly below.

      (1)   Annual costs (except for amortized investment)  for lime
           and  settle treatment were incurred to comply with  the
           promulgated  BPT  regulation.     These  coiists  were not
           included  in the current regulation if lime and  settle
           treatment is in place.

      (2)   Chemical precipitation costs were  based on lime  addi-
           tion  except  for  plants that  currently utilize  sodium
           hydroxide  or   soda  ash.     In  these  cases,    sodium
           hydroxide addition was  assumed for  cost estimation.

      (3)   Activated carbon adsorption  was  included as  a  prelimi-
           nary  treatment  step  for   delacquering scrubber  blow-
           down to  control  phenolics.   Analytical data supplied to
           the  Agency  indicate  TSS  concentrations were small  enough
           not   to   cause plugging, so  pretreatment  prior  to  enter-
           ing  the  column was  unnecessary.

      (4)   Ammonia   steam stripping was included  as  a  preliminary
           treatment   step  for  dross washing.    Since   the   steam
           requirements  for  such treatment may exceed the  excess
           steam  generation  capacity of  a given   plant,  a   steam
           generation  unit was  included in the costs.

      (5)   The ingot  conveyer casting contact cooling  water  was
routed   to    the   demagging   scrubber   operation    (if   this
operation   was   present),  and  the  costs  of    this   routing
were included.  When  demagging wet air pollution  control was  not
practiced  at  the plant, compliance          costs were based  on
90 percent recycle through cooling          towers.

    (6)   Recycle  of  air pollution control scrubber  liquor was
          based^ on recycle through holding tanks.   Annual costs
          associated  with  maintenance and sludge  disposal were
          included  in  the estimated  compliance  costs.   Spent
          activated  carbon was assumed to be regenerated or dis-
          posed  of  as  a hazardous waste  depending  on  volume
                               966

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         SECONDARY ALUMINUM SUBCATEGORY
SECT - VIII
          generated.   If  a  plant currently  recycles  scrubber
          liquor, capital costs of the recycle equipment (piping,
          pumps,  and  holding  tanks) were not included  in  the
          compliance  costs.

    (7)   Capital and annual costs for plants discharging in both
          the  secondary and primary aluminum subcategories  were
          based  on  a  combined treatment system and were appor-
          tioned to each subcategory on a flow-weighted basis.

NONWATER QUALITY ASPECTS

A  general  discussion  of the nonwater quality  aspects  of  the
control  and  treatment  options considered  for  the  nonferrous
metals  category  is  contained in Section VIII  of  the  General
Development Document.   Nonwater quality impacts specific to  the
secondary  aluminum  subcategory including  energy  requirements,
solid waste, and air pollution are discussed below.

ENERGY REQUIREMENTS

The methodology used for determining the energy requirements  for
the  various options is discussed in Section VIII of the  General
Development  Document.   Implementation of Option A technology is
estimated to require 2.4 MW-hr/yr,  while Option C would  require
2.5  MW-hr/yr  for  the  subcategory.   At  a  typical  secondary
aluminum  plant,  Option  A represents a 2.3 percent increase  in
overall  electrical consumption,  and Option C represents  a  2.4
percent  increase in overall electrical consumption.   Therefore,
it is concluded that the technology options considered will  have
a  minimal impact on energy consumption in the secondary aluminum
subcategory.

SOLID WASTE

Sludges  associated with the secondary aluminum subcategory  will
necessarily  contain  toxic  quantities (and  concentrations)  of
toxic  metal pollutants.   The Agency examined the  solid  wastes
that  would  be generated at secondary aluminum plants  by  lime,
settle,  and  filter treatment technologies and believes they are
not hazardous wastes under the Agency's regulations  implementing
Section 3001 of the Resource Conservation and Recovery Act.  None
of  these  wastes is listed specifically as hazardous.   Nor  are
they likely to exhibit a characteristic of hazardous  waste.   By
the  addition of excess lime during treatment,  similar  sludges,
specifically  toxic  metal bearing sludges,  generated  in  other
industrial   categories   such   as  the  iron  and   steel   and
electroplating categories,  passed the Extraction Procedure  (EP)
toxicity test.   See 40 CFR 8261.24.   Thus,  the Agency believes
that the wastewater sludges will similarly not be EP toxic if the
recommended technology is applied.

Certain  secondary  aluminum  plants  also  will  generate  spent
activated  carbon which will be contaminated with phenols.   Such
spent  carbon  is not listed as a hazardous waste  and  would  be
                               967

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          SECONDARY ALUMINUM SUBCATEGORY
SECT - VIII
 unlikely   to  exhibit  a  characteristic  of  hazardous   waste.
 Nevertheless,  the  Agency  has included costs for  disposing  of
 spent carbon as a hazardous waste,  or  (where volumes justify the
 practice)  of  regenerating it.   Spent carbon is  not  currently
 subject to RCRA regulation when stored before recycling.   See 40
 CFR S261.6(a).

 Although it is the Agency's view that solid wastes generated as a
 result  of  these  guidelines are not expected to  be  hazardous,
 generators  of these wastes must test the waste to  determine  if
 the  wastes  meet any of the characteristics of  hazardous  waste
 (see 40 CFR 262.11).

 If  these wastes should be identified or are listed as hazardous,
 they  will  come  within the scope of RCRA's  "cradle  to  grave"
 hazardous waste management program,  requiring regulation from the
 point  of  generation  to  point  of  final  disposition.    EPA's
 generator  standards require generators of  hazardous  nonferrous
 metals  manufacturing wastes to meet containerizatiori,  labeling,
 record keeping, and reporting requirements.  If plants dispose of
 hazardous  wastes  off-site,   they  are  required  to  prepare  a
 manifest  which  tracks  the  movement of  the  wastes  from  the
 generator's premises to a permitted  off-site treatment,   storage,
 or disposal facility.    See 40 CFR 262.20 (45 FR 33142,   May  19,
 1980,   as  amended  at 45 FR  86973,  December  31,   1980).    The
 transporter  regulations require transporters of hazardous wastes
 to comply with the manifest system to assure that the wastes  are
 delivered  to  a  permitted facility.   (See 40 CFR 263.20   45  FR
 33151,   May  19,   1980,   as amended  at 45 FR 86973,   December 31,
 1980).     Finally,   RCRA  regulations  establish  standards  for
 hazardous   waste   treatment,   storage,  and  disposal   facilities
 allowed   to receive  such wastes.    (See  40  CFR Part   264,   46  FR
 2802, January 12,  1981,  47  FR  32274, July 26,  1982).

 Even if  these  wastes are not  identified  as  hazardous,   they  still
 must_ be  disposed   of  in  compliance  with  the  Subtitle   D   open
 dumping  standards,   implementing 4004  of  RCRA.   (See  44 FR 53438>
 September  13,   1979).    The Agency has calculated  as part  of   the
 costs  for  wastewater  treatment  the  cost  of hauling and disposing
 of  these wastes.  The  Agency estimates implementation  of lime and
 settle   technology  will generate approximately 11,000  tons   per
 year  of wastewater treatment  sludge.  Treatment of  delacquering
 wet air  pollution control will generate approximately  177  pounds
 per year of spent carbon.  Multimedia  filtration technology   will
 not  result  in  any   significant  amount  of  sludge  over   that
 generated by lime precipitation.

 AIR POLLUTION

 There  is no reason to believe that  any substantial air pollution
problems  will  result   from  implementation  of  ammonia   steam
 stripping,  oil skimming,  chemical  precipitation, sedimentation,
and   multimedia   filtration.    These   technologies   transfer
pollutants to solid waste and do not involve air stripping or any
other  physical  process  likely to  transfer pollutants  to  air.
                               968

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         SECONDARY ALUMINUM SUBCATEGORY
SECT - VIII
Water  vapor containing some particulate matter will be  released
in the drift from the cooling tower systems which are used as the
basis  for flow reduction in the secondary aluminum  subcategory.
However,   the  Agency  does  not  consider  this  impact  to  be
significant.
                                969

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             SECONDARY ALUMINUM SUBCATEGORY
         SECT - VIII
                           Table VIII-1

    COST OF COMPLIANCE FOR THE SECONDARY ALUMINUM SUBCATEGORY

                        DIRECT DISCHARGERS*
         	Proposal	
Option   Capital Cost   Annual Cost

  A         2,000,000     1,800,000

  C         2,200,000     1,900,000
	Promulgation	
Capital Cost   Annual Cost

   1,000,000       600,000

   1,100,000       640,000
*1782 dollar
                              970

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             SECONDARY ALUMINUM  SUBCATEGORY
                                       SECT  - VIII
                           Table VIII-2
    COST OF COMPLIANCE FOR THE SECONDARY ALUMINUM SUBCATEGORY
                       INDIRECT DISCHARGERS*
Option
  A
  C
Capital Cost
   3,000,000
   3,300,000
                  Proposal
Annual Cost
  2,000,000
  2,200,000
Capital Cost
   2,100,000
   2,300,000
                                    Promulgation
Annual Cost
  1 ,300,000
  1,400,000
 *1982  dollars
                                971

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SECONDARY ALUMINUM SUBCATEGORY
SECT - VIII
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                     972

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          SECONDARY ALUMINUM SUBCATEGORY
SECT - IX
                            SECTION IX

     BEST PRACTICABLE CONTROL TECHNOLOGY CURRENTLY AVAILABLE
EPA  promulgated  best practicable control  technology  currently
available  (BPT) effluent limitations standards for the secondary
aluminum  industry on April 8,  1974 as Subpart C of 40 CFR  Part
421.   Pollutants  regulated  by these  standards  are  aluminum,
copper,  chemical oxygen demand,  ammonia, fluoride, TSS, and pH.
Unlike  the current rulemaking,  the BPT standards were developed
on  the  basis  of two subdivisions  of  the  secondary  aluminum
process,  not  on  the basis of segments that isolate  individual
wastewater streams.  BPT standards were established for magnesium
removal  processes (demagging using either chlorine  or  aluminum
fluoride)  and wet residue processes.   The effluent  limitations
established by the 1974 BPT standards also require zero discharge
of metal cooling water.

     (a)  The  following  limitations establish the  quantity  or
          quality  of pollutants or pollutant  properties,  which
          may  be  discharged  by a point source subject  to  the
          provisions  of  this subpart and which uses  water  for
          metal  cooling,  after application of the best  practi-
          cable  control technology currently  available:   There
          shall be no discharge of process wastewater  pollutants
          to navigable waters.

     (b)  The  following  limitations establish the  quantity  or
          quality of pollutants or pollutant properties which may
          be  discharged by a point source subject to the  provi-
          sions  of this subpart and which uses aluminum fluoride
          in its magnesium removal process ("demagging process"),
          after  application  of  the  best  practicable  control
          technology  currently  available:   There shall  be  no
          discharge  of  process wastewater pollutants  to  navi-
          gable waters.

     (c)  The  following  limitations establish the  quantity  or
          quality  of  pollutants or  pollutant  properties  con-
          trolled  by  this section,  which may be discharged  by
          a  point  source  subject to  the  provisions  of  this
          subpart  and  which  uses  chlorine  in  its  magnesium
          removal   process,   after  application  of  the   best
          practicable control technology currently available:
                               973

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          SECONDARY ALUMINUM SUBCATEGORY
                         SECT - IX
                               Effluent Limitations
   Effluent
Characteristic
Average of daily values for 30 consecutive
           days shall not exceed
                   Metric units  (kilograms per 1,000 kg
                             magnesium removed)
                   English units  (Ibs per 1,000 Ibs
                             magnesium removed)

TSS                                  175
COD                                    6.5
pH                        Within  the range of 7.5 to 9.0

     (d)  The  following  limitations establish the  quantity  or
          quality  of  pollutants or pollutant  properties  which
          may  be  discharged  by a point source subject  to  the
          provisions  of this subpart and which  processes  resi-
          dues  by  wet methods/  after application of  the  best
          practical control technology currently available:

                               Effluent Limitations
   Effluent
Characteristic
Average of daily values for 30 consecutive
           days shall not exceed
TSS
Fluoride-
Ammonia (as N)
Aluminum
Copper
COD
pH
Metric units (kilograms per 1,000 kg
          magnesium removed)
English units (Ibs per 1,000 Ibs
          magnesium removed)

                    1.5
                    0.4
                    0.01
                    1.0
                    0.003
                    1.0
      Within the range of 7.5 to 9.0
                               974.

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           SECONDARY  ALUMINUM SUBCATEGORY    SECT  -  X



                            SECTION X

        BEST AVAILABLE TECHNOLOGY ECONOMICALLY ACHIEVABLE


The  effluent  limitations  are based on  the  best  control  and
treatment  technology used by a specific point source within  the
industrial category or subcategory,  or by another  industry where
it  is  readily transferable.   Emphasis is placed  on  additional
treatment techniques applied at the end of the treatment  systems
currently  used  for BPT,  as well as reduction of  the amount  of
wate? 'used  and  discharged,   process  control,  and  treatment
technology optimization.

The  factors  considered in assessing best  available  technology
economically  achievable (BAT) include the age of  equipment  and
facilities involved,  the process used, process changes, nonwater
quality  environmental  impacts  (including energy  requirements),
and  the costs of application of such technology (Section  304(b)
<2)(B) of the Clean Water Act).  At a minimum, BAT represents the
best  available technology economically achievable at  plants  of
various ages,  sizes, processes, or other characteristics J-  Where
the  Agency  has found  the existing performance to  be  uniformly
inadequate!  BAT  may be transferred from a different subcategory
or  category.   BAT  may  include  feasible  process  changes  or
internal controls, even when  not in common  industry practice.
The
      required  assessment of BAT considers costs,  but  does   not
      re^ balancing of costs against effluent  reduction  benefits
 (see  Weyerhaeuser  v.  Costle,   590 F.2d.  1011 (D.C. Cir .  1978)).
 However!  in   assessing"" the" proposed BAT,   the Agency has given
 substantial    weight  to  the   economic   achievability   of    the
 technology.

 On April  8,   1974, EPA promulgated  technology-based BAT effluent
 limitations   guidelines for the secondary aluminum  subcategory.
 BAT  required  zero   discharge based on  100  percent   recycle  of
 casting  contact  cooling  water   and   in-process  changes which
 eliminate demagging wet air pollution  control  and  residue  filling
 (dross washing).  Elimination  of  demagging scrubbers was based on
 the  installation of  the Durham process,  ALCOA process,  and   the
 Teller   process,  which   significantly   reduces   fuming    during
 demaqqing  and the need  for wet scrubbers.   The Agency  believed
 tha?  each  of these processes  was sufficiently well   demonstrated
 to  be installed and  become operational  by   1984.    Consequently,
 there  was  no justification  for a discharge  allowance   associated
 with this waste stream.   However, new information  shows  that   the
 technologies  are  not   sufficiently demonstrated   nor  are  they
 applicable  to plants  on a nationwide basis.

 A similar situation  exists for dross washing.   Zero discharge for
 this  operation  was   based on demonstrated  dry  milling  in  the
 subcategory.   However,  the extensive retrofits of installing dry
 milling  have  prompted EPA to reevaluate the existing  BAT  zero
                                975

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             SECONDARY ALUMINUM  SUBCATEGORY   SECT - X


  discharge  requirement.   For these reasons,  the existing BAT  is
  modified   to  allow a discharge for demagging wet  air  pollution
  control and dross washing.

  TECHNICAL  APPROACH TO BAT

  In  pursuing  this  second round  of  effluent  regulations,  EPA
  reviewed   a  wide range of technology options and  evaluated  the
  available  possibilities  to ensure that the most  effective  and
  beneficial  technologies  were  used as the  basis  of  BAT.   To
  accomplish  this,  the Agency elected to examine  two  technology
  alternatives  which  could be applied to the  secondary  aluminum
  subcategory as BAT options.
 In  summary,  the treatment technologies considered for
 presented below:

 Option A (Figure X-l, page 995) is based on
                                                     BAT  are
      o  Preliminary treatment with oil skimming (where required)
      o  Preliminary treatment of dross washing wastewater with
         ammonia steam stripping
      o  Preliminary treatment of delacquering wet air pollution
         control wastewater with activated carbon adsorption
      o  In-process flow reduction of casting contact cooling
         water and scrubber liquor resulting from scrap drying and
         delacquering wet air pollution control
      o  Chemical precipitation and sedimentation

 Option C (Figure X-2,  page 996)  is based on

         Preliminary treatment with oil skimming (where required)
         Preliminary treatment of dross washing wastewater with
         ammonia steam  stripping
         Preliminary treatment of delacquering wet  air pollution
         control wastewater with  activated carbon adsorption
         In-process  flow reduction of casting contact  cooling
         water  and scrubber liquor resulting from scrap drying and
         delacquering wet  air  pollution control
         Chemical  precipitation and sedimentation
         Multimedia  filtration
o
o
o
o
The  two  options for BAT are discussed in greater detail  below.
The first option considered is analogous to the BPT treatment and
control technology.


OPTION A

Option A requires control and treatment techologies to reduce the
discharge  of  wastewater  volume  and  pollutant  mass.    These
measures include in-process changes, resulting in the elimination
of  some wastewater streams and the concentration  of  pollutants
in other effluents.   As explained in Section VII of the  General
Development  Document,  treatment of a more concentrated effluent
                               976

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           SECONDARY ALUMINUM SUBCATEGORY   SECT - X
allows  achievement  of  a  greater  net  pollutant  removal  and
introduces   the  possible  economic  benefits  associated   with
treating a lower volume of wastewater.   Methods used in Option A
to  reduce  process  wastewater  generation  or  discharge  rates
include the following:

Recycle of Casting Contact Cooling Water

The  function  of  casting contact cooling water  is  to  quickly
remove heat from the newly formed ingot or bar.   Therefore,  the
principal  requirements of the water are that it be cool and  not
contain  dissolved  solids  at a concentration that  would  cause
water marks or other surface imperfections.   There is sufficient
category  experience with casting contact cooling wastewaters  to
assure  the  success of this technology using cooling  towers  or
heat exchangers (refer to Section VII of the General  Development
Document).   A  blowdown  or  periodic cleaning is likely  to  be
needed  to prevent a build-up of dissolved and suspended  solids.
(EPA  has determined that a blowdown of 10 percent of  the  water
applied in a process is adequate.)

Reuse of casting contact cooling water is also an effective means
of   reducing  flow.    One  plant  in  the  secondary   aluminum
subcategory has demonstrated that ingot conveyer casting  contact
cooling water can be reused as demagging scrubber liquor make-up.
EPA  knows of no engineering reason why this water is  unsuitable
for make-up water to the demagging scrubber.

Recycle of Water Used in Wet Air Pollution Control

There  are  three  wastewater  sources associated  with  wet  air
pollution  control  which  are  regulated  under  these  effluent
limitations:

     1.  Delacquering,
     2.  Scrap drying, and
     3.  Demagging.

Table  X-l  (page  987)presents the number  of  plants  reporting
wastewater   use  with  these  sources,  the  number  of   plants
practicing  recycle of scrubber liquor, and the range of  recycle
values being used.

The Option A treatment model  includes in-process flow reduction,
steam  stripping  and  activated  carbon  adsorption  preliminary
treatment  of  wastewaters containing ammonia  and  phenolics  at
treatable  concentrations  and  oil  skimming,   where  required.
Preliminary  treatment is followed by chemical precipitation  and
sedimentation  (see  Figure  X-l, page 987).   Although  oil  and
grease is a conventional pollutant limited under best practicable
technology (BPT), oil skimming is needed for BAT to ensure proper
metals  removal.   Oil and grease interferes  with  the  chemical
addition   and   mixing  required  for   chemical   precipitation
treatment.   Chemical precipitation is used to remove  metals  by
the   addition  of  lime  followed  by   gravity   sedimentation.
                               977

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           SECONDARY ALUMINUM SUBCATEGORY   SECT - X


Suspended solids are also removed from the process.

OPTION C

Option  C for the secondary aluminum subcategory builds upon  the
Option  A  control  and treatment technology of  in-process  flow
reduction,   oil   skimming  (where  required),   ammonia   steam
stripping,  activated carbon adsorption,  chemical precipitation,
and  sedimentation by adding multimedia filtration technology  at
the  end of the Option A treatment scheme (see Figure  X-2,  page
988).  Multimedia filtration is used to remove suspended  solids,
including  precipitates  of  metals,  beyond  the   concentration
attainable by gravity sedimentation.  The filter suggested is  of
the  gravity, mixed media type, although other forms of  filters,
such  as  rapid sand filters or pressure filters,  would  perform
satisfactorily.

INDUSTRY COST AND POLLUTANT REMOVAL ESTIMATES

As  a means of evaluating each technology option,  EPA  developed
estimates  of the pollutant removal estimates and the  compliance
costs  associated  with  each  option.    The  methodologies  are
described below.

POLLUTANT REMOVAL ESTIMATES

A  complete description of the methodology used to calculate  the
estimated  pollutant reduction achieved by the application of the
various  treatment  options  is presented in  Section  X  of  the
General  Development Document.   The pollutant removal  estimates
have  been revised from proposal based on comments and new  data.
However,  the  methodology for calculating pollutant removals has
not changed.  The data used for estimating pollutant removals are
the same as those used to revise the compliance costs.

Sampling  data  collected during the field sampling program  were
used  to  characterize  the major waste  streams  considered  for
regulation.   At  each sampled facility,  the sampling data  were
production  normalized  for each unit operation  (i.e.,  mass  of
pollutant  generated  per mass of  product  manufactured).   This
value,  referred  to as the raw waste,  was used to estimate  the
mass of toxic pollutants generated within the secondary  aluminum
subcategory.  By multiplying the total subcategory production for
a  unit operation by the corresponding raw waste value,  the mass
of pollutant generated for that unit operation was estimated.

The volume of wastewater discharged after the application of each
treatment  option was estimated for each operation at each  plant
by  comparing the actual discharge to the regulatory  flow.   The
smaller  of  the two values was selected and  summed  with  other
plant flows.  The mass of pollutant discharged was then estimated
by  multiplying the achievable concentration values attainable by
the  option (mg/1) by the estimated volume of process  wastewater
discharged by the subcategory.   The mass of pollutant removed is
simply  the  difference between the estimated mass  of  pollutant
                               978

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           SECONDARY ALUMINUM SUBCATEGORY
SECT - X
generated  within  the  subcategory and  the  mass  of  pollutant
discharged after application of the treatment option.   Pollutant
removal  estimates for the secondary aluminum direct  dischargers
are presented in Table X-2 (page 988).

COMPLIANCE COSTS

Compliance costs presented at proposal were estimated using  cost
curves,   which   related   the  total  costs   associated   with
installation  and operation of wastewater treatment  technologies
to plant process wastewater discharge.   EPA applied these curves
on  a  per  plant  basis,  a plant's  costs  (both  capital,  and
operating and maintenance) being determined by what treatment  it
has  in-place and by its individual process wastewater  discharge
(from  dcp).  The final step was to annualize the capital  costs,
and  to sum the annualized capital costs,  and the operating  and
maintenance  costs,  yielding  the  cost of  compliance  for  the
subcategory.

Since proposal,  the cost estimation methodology has been changed
as  discussed in Section VIII of this supplement. A design  model
and  plant-specific  information were used to size  a  wastewater
treatment system for each discharging facility.  After completion
of  the design, capital and annual costs were estimated for  each
unit  of the wastewater treatment system.  Capital costs rely  on
vendor  quotes,  while  annual  costs  were  developed  from  the
literature.  The revised compliance costs for direct  dischargers
are presented in Table VIII-1 (page 970).

BAT OPTION SELECTION

EPA   has  selected  Option  C  as  the  basis  of  BAT  in  this
subcategory.   The BAT treatment scheme proposed consists of flow
reduction,  oil skimming (where required),  preliminary treatment
of   ammonia   steam  stripping  and   activated   carbon,   lime
precipitation, sedimentation, and filtration for control of toxic
metals.   The  selected  option increases the  removal  of  toxic
pollutants from raw wastewater by approximately 9,600 kg/yr,  530
^9/yr   of   phenolics,   and   nonconventional   pollutants   by
approximately   90,800   kg/yr.    This   option   also   removes
approximately  8.2  kg/yr  of toxic pollutants and  36  kg/yr  of
nonconventional pollutants over the estimated BPT discharge.  The
estimated  capital  cost  of proposed BAT is $1.1  million  (1982
dollars) and the annual cost is $0.64 million (1982 dollars).

Ammonia steam stripping is demonstrated in the nonferrous  metals
manufacturing  category  by two plants in the primary  columbium-
tantalum  subcategory,  and three plants in the primary  tungsten
subcategory.    Activated  carbon  is  not  demonstrated  in  the
subcategory,  but it is a classic means of removing phenols  from
wastewater.

Activated   carbon  is  demonstrated  in  the  iron   and   steel
(cokemaking)  category  as  a phenols  removal  technology.   The
treatment  performance used for activated carbon to develop  mass
                               979

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            SECONDARY ALUMINUM SUBCATEGORY   SECT - X
 limitations   for   total  phenolics  is   based  on  the  attainable
 quantification limit  of  0.010  mg/1.    EPA believes  this  value  is
 achievable when adequate  quantities of  carbon are  used.

 At  the  source requirements  (i.e.,  requiring that  compliance   be
 demonstrated   and  monitoring conducted  prior to  commingling  with
 process   or   nonprocess  waters)  are promulgated  for  phenol   in
 delacquering   wet   air pollution control   wastewaters.   This   is
 because   there is  a distinct possibility that plants  may  be  able
 to meet  the limits for toxic organics through dilution  unless the
 compliance point is at-the-source,  rather  than end-of-pipe.  This
 is because the organic pollutants are present in wastewater  from
 only certain unit operations,  and  are  present at  concentrations
 that could be reduced  below  the analytical detection  levels after
 commingling   with  other process wastewaters.  The plants known   to
 currently operate  delacquering  scrubbers are principally  primary
 aluminum and  aluminum  forming plants, which generate  much larger
 volumes   of process wastewater  than the delacquering operation.
 Therefore, at-the-source  requirements are  promulgated to  prevent
 dilution.

 Carbon   adsorption  may require preliminary treatment to remove
 suspended  solids  and  oil and  grease.    Suspended   solids
 concentrations  in  the  influent should be reduced   to   minimize
 backwash requirements.   Four  sample  analyses  of   delacquering
 scrubber  liquor submitted to the Agency showed  suspended solids
 concentrations  of  22,  9.0, 17.2,  and 60.8  mg/1.

 These  concentrations  are essentially those achievable with  lime
 and  settle treatment (19.5 mg/1 ten day average).   Therefore,  it
 appears   pretreatment  for TSS is  not required prior to  activated
 carbon   adsorption pretreatment.   Oil  and grease data  were  not
 submitted.

 Since  filtration   removes additional toxic  and  nonconventional
 pollutants,  and   is economically achievable,  it is  included   as
 part  of  proposed  BAT.   Filtration also  adds to  the  treatment
 system   reliability  by making  it less  susceptible   to   operator
 error   and  to  sudden  changes  in  raw   wastewater  flows  and
 concentrations.    Further,    the  selection   of  filters  is    an
 appropriate  balance to the  elimination of  previously promulgated
 no  discharge  BAT  requirements for ingot   conveyer   casting  and
 dross washing.  Providing these two allowances is only  justified
when the Agency can assume that most of the pollutants  contained
 in these discharges will be  removed by  treatment.

For  the  Secondary Aluminum  Subcategory,   EPA  promulgated  final
amendments  on  July   7, 1987 (52 FR  25552)   to  the  regulation
concerning two topics,  which are described  here.

EPA  has amended the flow basis for two subdivisions based  on  a
re-evaluation of data available in the Administrative Record  for
this  rulemaking.    These  two subdivisions  are  ingot  conveyer
casting and demagging wet air pollution control.
                               980

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           SECONDARY ALUMINUM SUBCATEGORY   SECT - X
WASTEWATER DISCHARGE RATES

Specific   wastewater  streams  associated  with  the   secondary
aluminum   subcategory  are  generated  from  scrap  drying   air
pollution control,  scrap screening arid milling,  dross  washing,
demagging  wet  air  pollution  control,   delacguering  wet  air
pollution  control,  direct chill casting contact cooling,  ingot
conveyer  casting contact cooling, shot casting contact  cooling,
and stationary casting contact cooling.

Table  X-3 (page 989) lists the production normalized  wastewater
discharge  rates allocated at BAT for these  wastewater  streams.
The values represent the best existing practices of the industry,
as  determined from the analysis of dcps.   Individual  discharge
rates from the plants surveyed are presented in Section V of this
supplement for each wastewater stream.

SCRAP DRYING WET AIR POLLUTION CONTROL WASTEWATER

No  BAT  wastewater  discharge allowance was proposed  for  scrap
drying  air  pollution  control.   Only three of  29  plants  use
scrubbers  to  control emissions;  the remaining  26  plants  use
baghouses.   Two  of the three plants with scrubbers achieve zero
discharge  by 100 percent recycle.   One plant is a  once-through
discharger with a rate of 1,057 1/kkg (253.5 gal/ton) of aluminum
scrap  produced.  This  plant also reported that  it  planned  to
discontinue  the  use  of the  scrubber.   Wastewater  rates  are
presented in Section V (Table V-l,  page 912).  The BAT allowance
is   zero  discharge  of  wastewater  pollutants  based  on   the
attainment  of no discharge by 28 of 29 plants, including two  of
the three operations using wet air pollution control.  No data or
information  were  submitted  to the  Agency  demonstrating  zero
discharge as proposed is not attainable.

SCRAP SCREENING AND MILLING

No BAT wastewater discharge rate was proposed for scrap screening
and  milling.   Both  plants reporting this wastewater  are  zero
dischargers because of 100 percent recycle or reuse.   Therefore,
the  Agency  believes  that zero discharge is  possible  for  all
secondary  aluminum scrap screening and  milling  processes.   No
data  or information were submitted to the Agency demonstrating a
discharge allowance is needed for scrap screening and milling.

DROSS WASHING WASTEWATER

The  proposed  BAT  wastewater discharge rate  was  10,868  1/kkg
(2,607  gal/ton)  of  dross  processed.     Four  plants  reported
producing this wastewater.  Two plants discharge from the process
after 67 percent recycle.   One plant completely evaporates  this
wastewater.    The BAT rate is the discharge from plant 4104.  Two
plants  recycle  100  percent  of the  wastewater.   No  data  or
information  were submitted to the Agency demonstrating that  the
proposed discharge allowance was not appropriate;   therefore,  the
promulgated  discharge  rate  is equal  to  that  proposed.   EPA
                               981

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            SECONDARY ALUMINUM SUBCATEGORY
SECT - X
 considers  the zero discharge practices for this waste stream  to
 be  site-specific  and  not applicable  on  a  nationwide  basis.
 Wastewater  rates  for dross washing are presented in  Section  V
 (Table V-3r page 914).

 DEMAGGING WET AIR POLLUTION CONTROL

 The  proposed  BAT wastewater discharge rate was 800  1/kkg  (192
 gal/ton)  of aluminum demagged.   This rate is allocated only for
 plants^   practicing  wet  air  pollution  control  of   demagging
 operations.   Of  the 37 demagging operations  reported,  20  use
 water for emissions control.  Nine plants using water reported no
 wastewater discharge, achieved by recycle or reuse.   Eight of the
 nine  plants completely recycle the wastewater,  while one  plant
 did  not report a recycle percentage.    Another plant practices a
 partial  recycle of 40 percent.   Nine  plants were thought to have
 once-through  operations,  eight  of these discharging  223.3  to
 1,956.24  1/kkg  (54.5  to 469.2 gal/ton).   No  flow  data  were
 provided  by one of the discharging plants.    A  distribution  of
 wastewater   rates  considered  is  presented  in  the   proposed
 secondary  aluminum supplemental development document.   Industry
 comments prior to proposal asserted that the use of  recirculation
 systems    using   treated  water   reduces   demagging   scrubber
 efficiency.    Therefore,   recycle of scrubber liquor  was not used
 as   a  basis  for the BAT discharge rate for  demagging  wet  air
 pollution  control.    The  BAT  discharge rate was based  on  the
 average  of the nine discharging plants.

 Commenters  on  the  proposed   mass limitations questioned  the
 reported 100 percent  recycle of demagging scrubber liquor  in  the
 proposed   supplemental   development  document.    In   addition,
 commenters  questioned the calculation of the demagging  scrubber
 discharge  allowance.     Based  on  these comments,   the   Agency
 re-evaluated   the discharge rate for demagging  scrubber   liquor.
 Pour  plants   were   identified  and confirmed  to  achieve  zero
 discharge of demagging scrubber  liquor.   Zero discharge at   these
 plants is site-specific and not  appropriate  on a national   basis.
 A  blowdown  from  demagging scrubbers   is   required   to   control
 chloride   concentrations   in the scrubber  liquor.   Those   plants
 reporting   zero    discharge   recycle  from   ponds    with    large
 capacitites     and  they   may   also be   losing   water    through
 percolation.

 The most  predominant scrubber  used  for demagging  is the  Intecbell
 scrubber.   Three plants reported  using venturi  scrubbers and one
 plant  uses  a  packed tower.    Water  use   between   these   three
 scrubbers  is not significantly  different;   therefore,  all  data
 were considered together in selecting the BAT discharge rate. The
 promulgated   BAT  discharge   rate   was   697   1/kkg   of  aluminum
 demagged.  This   rate  represented  the average water use at   those
plants using less than 6,885 1/kkg.   Two plants were above  this
 rate,   and   they  were   not  considered  because  they  use  an
 inordinately large amount  of scrubber liquor when compared  to the
other plants.
                               982

-------
           SECONDARY ALUMINUM SUBCATEGORY
SECT - X
The  Agency  has  amended the flow rate  for  demagging  wet  air
pollution  control  upon which are based the BAT limitations  and
NSPS,  PSES, and PSNS for the demagging wet air pollution control
subdivision.   Secondary  aluminum petitioners claimed  that  the
control  flow allowance of 697 1/kkg was incorrect due to a  data
interpretation error regarding the number of scrubbers associated
with the water usage for one facility.  The Agency agrees that it
made  an  error  in this calculation and has adjusted  the  water
usage for this plant upwards.   As a result, the final regulatory
flow allowance is 771 1/kkg.

DELACQUERING WET AIR POLLUTION CONTROL

A  BAT  discharge rate has been added to account  for  wastewater
associated with wet scrubbing of air pollution generated  through
the  recycle of aluminum cans.   Five plants reported the use  of
this  scrubber as shown in Table V-7.   The BAT discharge rate is
based on the average reported discharge for plants 505,  313, and
4101.   Each  of these plants practices recycle of 97 percent  or
greater and uses a venturi scrubber.   The BAT discharge rate  is
80  1/kkg.   Plant 340 was not included in the average because it
uses a rotoclone scrubber.   Water discharged for plant 340  with
no recycle compares well with the plants practicing recycle.

DIRECT CHILL CASTING CONTACT COOLING WATER

The  BAT  wastewater  discharge rate  for  direct  chill  casting
contact cooling water was proposed as 1,999 1/kkg (479.4 gal/ton)
of  aluminum  cast.   Direct  chill  casting  practices  and  the
wastewater  discharge from this operation are similar in aluminum
forming,   primary  aluminum  reduction  and  secondary  aluminum
plants.    The  information  available  does  not  indicate  _ any
significant difference in the amount of water required for direct
chill  casting  in  primary  aluminum,   secondary  aluminum  and
aluminum  forming plants.  For this reason,  available wastewater
data  from  aluminum  forming and primary  aluminum  plants  were
considered together in establishing BPT effluent limitations.  No
data  for  direct  chill  casting  water  use  were  provided  by
secondary aluminum plants.

In all, 26 primary aluminum plants and 61 aluminum forming plants
have  direct chill casting operations.   Recycle of  the  contact
cooling  water  is  practiced at 30 aluminum  forming  and  eight
primary aluminum plants.   Of these,  eight plants indicated that
total  recycle  of  this stream made it  possible  to  avoid  any
discharge  of  wastewater;  however,  the majority of the  plants
discharge a bleed stream.   The discharge flow for this operation
was  based on the average of those plants practicing  50  percent
recycle or greater.

The  Agency was in error in this determination (as pointed out by
a  commenter  from  the aluminum industry)  as  it  considers  90
percent  recycle or greater BAT technology.    (See 48 FR at  7052,
Feb. 17, 1983).  Therefore, the BAT discharge allowance has  been
recalculated  based  on those plants  (both primary  aluminum  and
                               983

-------
            SECONDARY ALUMINUM SUBCATEGORY
SECT - X
 aluminum  forming)  that have recycle rates between  90  and  100
 percent.  The revised BAT discharge rate is thus 1,329 1/kkg (319
 gal/ton)  of  aluminum  cast.  Although  there  are  no  reported
 secondary  aluminum plants with direct chill casting, the  Agency
 will  promulgate  mass  limitations  for  this  segment.   It  is
 possible new or existing sources may install direct chill casting
 in the future.

 INGOT CONVEYER CASTING CONTACT COOLING WATER

 In  the proposed guidelines for this subcategory,  ingot  conveyer
 casting   was  considered  stationary  casting  because  of   the
 promulgated zero discharge for metal cooling in the existing  BPT
 and ^BAT  effluent limitations.  However,   information  and  data
 submitted to the Agency indicate zero discharge of ingot conveyer
 casting is not demonstrated except when the discharge is recycled
 to  a demagging air pollution scrubber.  Therefore,  a  discharge
 allowance  was provided in the promulgated regulation  for   ingot
 conveyer  casting.   The  discharge rate,   based  on  90 percent
 recycle, was 43 1/kkg (10.3 gal/ton) of aluminum cast.   This rate
 was based on the average water usage with  the exception of  plants
 309 and 326.   Data from these two plants were not  used because  of
 excessive  water  use as determined through comparison  with  the
 other plants.  Only those plants not operating demagging scrubbers
 are  provided the ingot conveyer casting allowance.   One hundred
 percent  reuse  of casting water or  demagging  scrubber make-up
 water is demonstrated at one secondary aluminum facility.

 The  Agency  has  amended  the  flow  rate  upon  which  the BAT
 limitations  and NSPS,  PSES,  and PSNS for  ingot conveyer casting
 are   based.    Petitioners  claimed  that   the  regulatory    flow
 allowance  of  43 1/kkg  was incorrect due to  data   interpretation
 mistakes and  because  the Agency unnecessarily excluded  the   water
 usage of plants  that  reported achieving zero discharge.   EPA has
 promulgated an amended  flow allowance of 67 1/kkg,  which is  based
 on   corrected   water  usage data from  five  plants   (these   data
 involving  water   usage  and  operating  schedules   which    were
 interpreted  incorrectly by the  Agency in  constructing   the   flow
 allowance  in   the final rule)  and  includes three   plants'   water
 usage  that  reported achieving zero  discharge.   This  is  consistent
 with  EPA's  methodology  employed  throughout  the  nonferrous  metals
 rulemaking,  where the  Agency typically  used water  usage at   zero
 discharge  plants  in  determining  what  degrees  of   flow   reduction
 represent BAT, PSES,  NSPS,  and PSNS.

 STATIONARY  CASTING CONTACT  COOLING  WATER

No  BAT wastewater  discharge  allowance  is provided  for  stationary
casting   cooling.   In   the   stationary  casting  method,  molten
aluminum  is  poured  into  cast  iron  molds  and   then  generally
allowed   to  air cool.   The Agency  is aware of the use of  spray
quenching   to   quickly  cool  the  surface of  the  molten  aluminum
once it is cast into  the molds; however, this water evaporates on
contact with the molten aluminum.   As such,  the Agency believes
that there is no basis  for a pollutant discharge allowance.
                               984

-------
           SECONDARY ALUMINUM SUBCATEGORY   SECT - X
SHOT CASTING CONTACT COOLING WATER

No  BAT  wastewater  discharge allowance;  is  provided  for  shot
casting contact cooling.  Through information requests the Agency
has   found   zero  discharge  of  shot  casting  cooling   water
demonstrated  at two secondary aluminum facilities (of  the  four
reporting  the  practice).   Both  of these  plants  reported  no
product quality constraints due to 100 percent recycle.  Based on
the  demonstrated zero discharge practices for shot casting,  the
promulgated  flow  allowance requires zero discharge  of  process
wastewater pollutants.

REGULATED POLLUTANT PARAMETERS

In  implementing the terms of the Clean Water Act  Amendments  of
1977,   the  Agency  placed  particular  emphasis  on  the  toxic
pollutants.   The  raw wastewater concentrations from  individual
operations and the subcategory as a whole were examined to select
certain pollutants and pollutant parameters for consideration for
limitation.    This  examination  and  evaluation,  presented  in
Section   VI,   concluded   that  10  pollutants  and   pollutant
parameters  are  present  in secondary  aluminum  wastewaters  at
concentrations  that  can  be effectively reduced  by  identified
treatment technologies.

However,  the  cost  associated  with analysis  for  toxic  metal
pollutants has prompted EPA to develop an alternative method  for
regulating  and  monitoring toxic pollutant discharges  from  the
nonferrous metals manufacturing category.  Rather than developing
specific  effluent mass limitations and standards for each of the
toxic  metals  found  in  treatable  concentrations  in  the  raw
wastewaters from a given  subcategory,  the Agency is promulgating
effluent mass limitations only for those pollutants generated  in
the  greatest  quantities  as  shown  by  the  pollutant   removal
estimate   analysis.    The  pollutants  selected  for   specific
limitation are listed below:

     122.  lead
     128.  zinc
           total phenols  (4-AAP)
           aluminum
           ammonia

By  establishing  limitations and standards for certain  toxic metal
pollutants,   dischargers  will attain the same degree  of   control
over   toxic metal pollutants as they would have been  required  to
achieve  had all  the  toxic metal pollutants been directly limited.

This   approach   is   justified  technically   since  the   treatable
concentrations   used for  lime precipitation  and  sedimentation
technology  are  based  on  optimized  treatment   for   concomitant
multiple metals  removal.  Thus, even though  metals have  somewhat
different  theoretical solubilities,  they will be  removed at  very
nearly  the same  rate in  a  lime precipitation  and  sedimentation
                                985

-------
           SECONDARY ALUMINUM SUBCATEGORY
SECT - X
treatment   system   operated  for   multiple   metals   removal.
Filtration as part of the technology basis is likewise  justified
because this technology removes metals non-preferentially.  Thus,
cadmium  is  excluded  from limitation on the basis  that  it  is
effectively controlled by the limitations developed for lead  and
zinc.

The  toxic  metal pollutants selected for specific limitation  in
the  secondary aluminum subcategory to control the discharges  of
toxic  metal  pollutants are lead and zinc.   Ammonia  and  total
phenolics are also selected for limitation since the methods used
to  control  lead and zinc are not effective in  the  control  of
ammonia and total phenolics.

In Section VI,  phenol was selected for further consideration for
limitation.   However, data submitted to the Agency are primarily
in the form of total phenolics.  Since phenol is contained in the
total  phenolics analysis, limitation of total phenols will  also
control the toxic pollutant phenol.

EFFLUENT LIMITATIONS

The treatable concentrations achievable by application of the BAT
treatment  are discussed in Section VII of this  supplement.  The
treatable  concentrations  (both  one  day  maximum  and  monthly
average  values) are multiplied by the BAT  normalized  discharge
flows summarized in Table X-3 (page 989) to calculate the mass of
pollutants  allowed  to be discharged per mass of  product.   The
results  of  these calculations in milligrams  of  pollutant  per
kilogram  of product represent the BAT effluent  limitations  and
are presented in Table X-4 (page 990) for each waste stream.
                               986

-------
           SECONDARY ALUMINUM SUBCATEGORY
                     SECT  -  X
                           Table X-1

     CURRENT RECYCLE  PRACTICES WITHIN THE SECONDARY ALUMINUM
                           SUBCATEGORY
     Waste Stream

Delacquering Wet Air
 Pollution Control

Scrap Drying Wet Air
  Pollution Control

Demagging Wet Air
  Pollution Control

Ingot Conveyor Casting

Shot Casting
 Number of
Plants With
Wastewater
    20


    17

     4
Number of
  Plants
Practicing
 Recycle
     2

     2
 Range of
 Recycle
Values (%)

 97 -  98


    100


 40 - 100


 50 -  96

    100
                              987

-------
               SECONDARY ALUMINUM SUBCATEGORY
                                                  SECT - X
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               SECONDARY  ALUMINUM SUBCATEGORY
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-------
           SECONDARY ALUMINUM SUBCATEGORY
          SECT - X
                            TABLE X-4

                BAT EFFLUENT LIMITATIONS FOR THE
                 SECONDARY ALUMINUM SUBCATEGORY
Scrap Drying Wet Air Pollution Control

Pollutant or                 Maximum for            Maximum for
Pollutant property	 any one day	monthly average
          Metric Units - mg/kg of aluminum scrap dried
     English Units - Ibs/million Ibs of aluminum scrap dried

 Cadmium                          0.000                  0.000
*Lead                             0.000                  0.000
*Zinc                             0.000                  0.000
*Aluminum                         0.000                  0.000
*Ammonia (as N)                   0.000                  0.000

*Regulated Pollutant
Scrap Screening and Milling


Pollutant or                 Maximum for            Maximum for
Pollutant property	any one day	monthly average
   Metric Units - mg/kg of aluminum scrap screened and milled
English Units-lbs/million Ibs of aluminum scrap screened and milled
 Cadmium
*Lead
*Zinc
*Aluminum
*Ammonia (as N)

*Regulated Pollutant
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
                               990

-------
           SECONDARY ALUMINUM SUBCATEGORY
               SECT - X
                      TABLE X-4 (Continued)

                BAT EFFLUENT LIMITATIONS FOR THE
                 SECONDARY ALUMINUM SUBCATEGORY
Dross Washing
Pollutant or
Pollutant property
Maximum for
any one day
  Maximum for
monthly average
          Metric Units - mg/kg of aluminum dross washed
    English Units - Ibs/million Ibs of aluminum dross washed
 Cadmium
*Lead
*Zinc
*Aluminum
*Ammonia (as N)

*Regulated Pollutant
     2.174
     3.043
    11.090
    66.400
  1449.000
       0.869
       1.413
       4.565
      29.450
     636.900
Demagging Wet Air Pollution Control
Pollutant or
Pollutant property
Maximum for
any one day
  Maximum for
monthly average
         Metric Units - mg/kg of aluminum scrap demagged
   English Units - Ibs/million Ibs of aluminum scrap demagged
 Cadmium
*Lead
*Zinc
*Aluminum
*Ammonia (as N)

*Regulated Pollutant
     0.139
     0.195
     0.711
     4.250
    92.910
       0.056
       0.091
       0.293
       1.889
       40.850
                                991

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            SECONDARY ALUMINUM SUBCATEGORY   SECT - X
                       TABLE X-4 (Continued)

                 BAT EFFLUENT LIMITATIONS FOR THE
                  SECONDARY ALUMINUM SUBCATEGORY
 Delacquering Wet Air Pollution Control
 Pollutant or
 Pollutant property
       Maximum for
       any one day
                   Maximum for
                 monthly average
          _Metric Units - mg/kg of aluminum delacquered
      English Units - Ibs/million Ibs  of  aluminum delacquered
  Cadmium
 *Lead
 *Zinc
 *Aluminum
 *Ammonia (as  N)
 *Total Phenols(4-AAP)

 *Regulated Pollutant
 **At  the source
**
 0.016
 0.022
 0.082
 0.489
10.670
 0.001
                                   0.006
                                   0.010
                                   0.034
                                   0.217
                                   4.688
Direct Chill Casting Contact Cooling
Pollutant or
Pollutant property
       Maximum for
       any  one day
                   Maximum for
                monthly  average
              Metric Units - mg/kg of aluminum cast
        English Units - Ibs/million Ibs of aluminum cast
 Cadmium
*Lead
*Zinc
*Aluminum
*Ammonia (as N)

*Regulated Pollutant
            0.266
            0.372
            1.356
            8.120
         177.200
                        0.106
                        0.173
                        0.558
                        3.602
                      77.880
                               992

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           SECONDARY ALUMINUM SUBCATEGORY
                                 SECT - X
                      TABLE X-4 (Continued)

                BAT EFFLUENT LIMITATIONS FOR THE
                 SECONDARY ALUMINUM SUBCATEGORY
Ingot Conveyer Casting Contact Cooling (When Chlorine Demagging
—Air Pollution Control is Not Practiced On-Site)
Pollutant or
Pollutant property
                  Maximum for
                  any  one day
                      Maximum for
                     monthly  average
              Metric Units - mg/kg of aluminum cast
        English Units - Ibs/million Ibs of aluminum cast
 Cadmium
*Lead
*Zinc
*Aluminum
*Ammonia (as N)

*Regulated Pollutant
                        0.009
                        0.012
                        0.044
                        0.263
                        5.732
                            0.003
                            0.006
                            0.018
                            0.117
                            2.520
 Ingot Conveyor  Casting  Contact  Cooling (When Chlorine Demagging
 —^~    Air  Pollution Control is  Practiced On-Site)
 Pollutant
 Pollutant
or
property
Maximum for
any one day
  Maximum for
monthly average
       .1.1^ y./ JL W^/^. .i. ^JT	   -""-*  		*.	—	,   	-j—
       Metric Units - mg/kg of aluminum screened & milled
   English Units - Ibs/million Ibs of aluminum screened & milled
  Cadmium
 *Lead
 *Zinc
 *Aluminum
 *Ammonia (as N)

 *Regulated Pollutant
                        0.000
                        0.000
                        0.000
                        0.000
                        0.000
                            0.000
                            0.000
                            0.000
                            0.000
                            0.000
                                993

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            SECONDARY ALUMINUM SUBCATEGORY   SECT - X
                       TABLE X-4 (Continued)

                 BAT EFFLUENT LIMITATIONS FOR THE
                  SECONDARY ALUMINUM SUBCATEGORY
 Stationary Casting Contact  Cooling
 Pollutant  or
 Pollutant  property
Maximum  for
any one  day
  Maximum  for
monthly average
               Metric  Units  - mg/kg  of  aluminum  cast
         English  Units -  Ibs/million Ibs  of aluminum cast
  Cadmium
 *Lead
 *Zinc
 *Aluminum
 *Ammonia  (as N)

 *Regulated Pollutant
     0.000
     0.000
     0.000
     0.000
     0.000
       0.000
       0.000
       0.000
       0.000
       0.000
Shot Casting Contact Cooling


Pollutant or
Pollutant property
Maximum for
any one day
  Maximum for
monthly average
              Metric Units - mg/kg of aluminum cast
        English Units - Ibs/million Ibs of aluminum cast
 Cadmium
*Lead
*Zinc
*Aluminum
*Ammonia (as N)

*Regulated Pollutant
     0.000
     0.000
     0.000
     0.000
     0.000
       0.000
       0.000
       0.000
       0.000
       0.000
                               994

-------
SECONDARY  ALUMINUM SUBCATEGORY
SECT  - X
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-------
SECONDARY ALUMINUM SUBCATEGORY
SECT - X
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-------
          SECONDARY ALUMINUM SUBCATEGORY
                                   SECT - XI
                            SECTION XI

                 NEW SOURCE PERFORMANCE STANDARDS
The  basis  for  new source performance  standards  (NSPS)  under
Section  306  of  the  Act is  the  best  available  demonstrated
technology (BDT).    New plants have the opportunity to design the
best  and  most  efficient production  processes  and  wastewater
treatment  technologies,  without  facing  the  added  costs  and
restrictions  encountered  in  retrofitting  an  existing  plant.
Therefore,   Congress   directed   EPA  to  consider   the   best
demonstrated process changes,  in-plant controls, and end-of-pipe
treatment  technologies  which  reduce pollution to  the  maximum
extent feasible.

This  section  describes the control technology for treatment  of
wastewater   from  new  sources  and  presents   mass   discharge
limitations  of  regulatory pollutants for NSPS in the  secondary
aluminum subcategory, based on the described control technology.

TECHNICAL APPROACH TO BDT

All  of  the  treatment technology options applicable  to  a  new
source were previously considered for the BAT options.   For this
reason, two options were considered for BDT, all identical to the
BAT options discussed in Section X.   The treatment  technologies
used for the two BDT options are:

OPTION A

     o  Preliminary treatment with oil skimming  (where required)
     o  Preliminary treatment of delacquering wet air pollution
        control wastewater with activated carbon adsorption
     o  In-process flow reduction of casting contact cooling
        water and scrubber liquor resulting from scrap drying and
        delacquering wet air pollution control
     o  Chemical precipitation and sedimentation
OPTION C

     o
     o
      o
      o
Preliminary treatment with oil skimming (where required)
Preliminary treatment of delacquering wet air pollution
control wastewater with activated carbon adsorption
In-process flow reduction of casting contact cooling
water and scrubber liquor resulting from scrap drying and
delacquering wet air pollution control
Chemical precipitation and sedimentation
Multimedia filtration
                                997

-------
           SECONDARY  ALUMINUM SUBCATEGORY
SECT - XI
 Partial   or   complete   reuse   and  recycle   of   wastewater   is   an
 essential part  of  each  option.   Reuse  and  recycle  can  precede  or
 follow  end-of-pipe  treatment.    A more detailed   discussion   of
 these  treatment options is  presented  in Section X.

 BDT  OPTION SELECTION

 EPA  promulgated  the best  available  demonstrated technology  for
 the  secondary aluminum  subcategory on April 8,   1974 as Subpart C
 of 40  CFR Part  421.  The promulgated  NSPS prohibits the discharge
 of process wastewater except  for an allowance,   if  determined   to
 be   necessary,   which allows  the discharge  of process   wastewater
 from chlorine demagging.    In this respect,  promulgated NSPS was
 less  stringent than   promulgated BAT.    The   Agency   did this
 recognizing   that   NSPS   became  effective on the    date    of
 promulgation  and  did not believe  that  the  dry  chlorine demagging
 processes were  immediately  available.   The Agency  believed that
 they  were appropriate  for  BAT with its compliance  date being   10
 years  later.

 In February of  1983,  EPA proposed to modify the promulgated NSPS
 to allow for  a  discharge from chlorine  demagging and direct chill
 casting.   The   technology  basis  was identical  to  that of  the
 proposed  BAT treatment consisting of in-process flow   reduction,
 preliminary   treatment  by  oil  skimming and ammonia   steam
 stripping,  lime  precipitation,   sedimentation,  and   filtration
 (Option  C).

 With  the exception   of   dross   washing,   the modified   NSPS
 promulgated   for the secondary aluminum subcategory is  equivalent
 to the BAT technology.   Dross washing is not provided a discharge
 allowance in  the NSPS due to  the demonstration of dry milling   in
 the  subcategory.   In the 1974 development  document for secondary
 aluminum,  it   is  stated   that 17 of the   23  plants   processing
 residues   (drosses) practice  dry milling to  eliminate wastewater.
 Impact  mills,  grinders,   and screening operations cire used   to
 remove   the metallic aluminum values  from the nonmetcillic values.
 Dry  milling  is  not required for existing  sources  due to  the
 extensive  retrofits of  installing  mills,  grinders, amd screening
 operations.   New sources,  however,  have  the ability  to install
 the  best  equipment  without  the  costs   of  major    retrofits.
 Therefore, dry milling  is considered  appropriate for new sources.
 For  the  remaining waste  streams, the  Agency  believes that BAT,  as
 promulgated,  is  the best  demonstrated  technology.    Additional
 flow reduction and more stringent treatment technologies are not
 demonstrated  or readily transferable to the  secondary aluminum
 subcategory.

 REGULATED  POLLUTANT PARAMETERS

 The Agency has no reason to believe that the pollutants  that will
 be   found  in  treatable concentrations in processes  within  new
 sources  will  be  any  different  than  with  existing  sources.
Accordingly,  pollutants  and pollutant parameters  selected  for
 limitation  under  NSPS,  in  accordance with  the  rationale   of
                               998

-------
          SECONDARY ALUMINUM SUBCATEGORY
SECT - XI
Sections VI and X,   are identical to those selected for BAT.  The
conventional pollutant parameters TSS,  oil and grease, and pH are
also selected for limitation.

NEW SOURCE PERFORMANCE STANDARDS

The  NSPS discharge flows for  each wastewater source are the same
as the discharge rates for all the BAT options and are  presented
in  Table XI-1 (page 1000).  The mass of pollutant allowed to  be
discharged  per mass of product is calculated by multiplying  the
appropriate achievable treatment concentration by the  production
normalized  wastewater  discharge  flows  (1/kkg).   New   source
performance  standards  for the  secondary  aluminum  subcategory
waste streams are presented in Table XI-2 (page 1001).
                                999

-------
                   SECONDARY ALUMINUM SUBCATEGORY
                  SECT  - XI
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-------
          SECONDARY ALUMINUM SUBCATEGORY
               SECT - XI
                           TABLE XI-2

           NSPS FOR THE SECONDARY ALUMINUM SUBCATEGORY
Scrap Drying Wet Air Pollution Control
Pollutant or
Pollutant property
Maximum for
any one day
  Maximum for
monthly average
          ^/ i. v^f~r*•» •*• **_y       	;	.£	  -*• 	      •:-	;	^~
          Metric Units - mg/kg of aluminum scrap dried
     English Units - Ibs/million Ibs of aluminum scrap dried
 Cadmium
*Lead
*Zinc
*Aluminum
*Ammonia (as N)
*Oil and Grease
*TSS
*pH

*Regulated Pollutant
     0.000                  0.000
     0.000                  0.000
     0.000                  0.000
     0.000                  0.000
     0.000                  0.000
     0.000                  0.000
     0.000                  0.000
  Within the range of  7.0  to  10.0
            at all times
Scrap Screening and Milling

Pollutant or
Pollutant property
Maximum  for
any  one  day
  Maximum for
monthly  average
      Metric Units - mg/kg  of aluminum screened and milled
 English Units -  Ibs/million Ibs  of  aluminum screened and milled
 Cadmium
 *Lead
 *Zinc
 *Aluminum
 *Ammonia  (as  N)
 *Oil and Grease
 *TSS
 *pH

 *Regulated Pollutant
      0.000                   0.000
      0.000                   0.000
      0.000                   0.000
      0.000                   0.000
      0.000                   0.000
      0.000                   0.000
      0.000                   0.000
   Within the range of 7.0 to 10.0
             at all times
                                1001

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           SECONDARY ALUMINUM SUBCATEGORY
                SECT  -  XI
                       TABLE XI-2 Continued)

            NSPS FOR THE SECONDARY ALUMINUM SUBCATEGORY
 Dross Washing

 Pollutant  or
 Pollutant  property
Maximum for
any one day
  Maximum  for
monthly average
           Metric  Units  -  mg/kg  of  aluminum dross  washed
     English  Units -  Ibs/million Ibs  of  aluminum dross washed
  Cadmium
 *Lead
 *Zinc
 *Aluminum
 *Ammonia (as N)
 *Oil and Grease
 *TSS
 *pH

 *Regulated Pollutant
     0.000
     0.000
     0.000
     0.000
     0.000
     0.000
     0.000
       0.000
       0.000
       0.000
       0.000
       0.000
       0.000
       0.000
  Within the range of 7.0 to 10.0
            at all times
Demagging Wet Air Pollution Control
Pollutant or
Pollutant property
Maximum for
any one day
  Maximum for
monthly average
            Metric Units - mg/kg of aluminum demagged
      English Units - Ibs/million Ibs of aluminum demagged
 Cadmium
*Lead
*Zinc
*Aluminum
*Ammonia (as N)
*Oil and Grease
*TSS
*pH

*Regulated Pollutant
     0.139                  0.056
     0.195                  0.091
     0.711                  0.293
     4.250                  1.889
    92.910                 40.850
     6.970                  6.970
    10.460                  8.364
  Within the range of 7.0 to 10.0
            at all times
                               1002

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          SECONDARY ALUMINUM SUBCATEGORY
                                 SECT - XI
                      TABLE XI-2 Continued)

           NSPS FOR THE SECONDARY ALUMINUM SUBCATEGORY
Delacquering Wet Air Pollution Control
Pollutant or
Pollutant propert
                  Maximum for
                  any  one day
                       Maximum for
                     monthly average
          ±"- wyw J. "J	  	-t	j-*	-	-	-=-
          Metric Units - mg/kg of aluminum delacquered
     English Units - Ibs/million Ibs of aluminum delacquered
 Cadmium
*Lead
*Zinc
*Aluminum
*Ammonia (as N)
*Total Phenols(4-AAP)
*0il and Grease
*TSS
*pH

*Regulated Pollutant
**At the source
                        0.016                   0.006
                        0.022                   0.010
                        0.082                   0.034
                        0.489                   0.217
                       10.670                   4.688
                        0.001                    	
                        0.800                   0.800
                        1.200                   0.960
            Within the range of 7.0 to 10.0
                            at all time
Direct Chill Casting Contact Cooling
Pollutant
Pollutant
or
propert;
Maximum for
any one day
  Maximum for
monthly average
              Metric Units - mg/kg of aluminum cast
        English Units - Ibs/million Ibs of aluminum cast
 Cadmium
 *Lead
 *Zinc
 *Aluminum
 *Ammonia (as N)
 *Oil and Grease
 *TSS
 *pH

 *Regulated  Pollutant
                        0.266
                        0.372
                        1.356
                        8.120
                      177.200
                       13.290
                       19.940
                     Within the range of 7.0 to 10.0
                               at all times
                             0.106
                             0.173
                             0.558
                             3.602
                            77.880
                            13.290
                            15.950
                                1003

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           SECONDARY ALUMINUM SUBCATEGORY
                SECT - XI
                       TABLE XI-2 Continued)

            NSPS FOR THE SECONDARY ALUMINUM SUBCATEGORY
 Ingot Conveyer Casting Contact Cooling (When Chlorine
     Demagging Wet Air Pollution Control is Not Practiced On-Site)
 Pollutant or
 Pollutant property
 Maximum for
 any  one day
   Maximum for
monthly  average
               Metric Units - mg/kg of aluminum cast
         English Units - Ibs/million Ibs of aluminum  cast
  Cadmium
 *Lead
 *Zinc
 *Aluminum
 *Ammonia (as  N)
 *0il  and Grease
 *TSS
 *pH

 *Regulated Pollutant
      0.009                   0.003
      0.012                   0.006
      0.044                   0.018
      0.263                   0.117
      5.732                   2.520
      0.430                   0.430
      0.645                   0.516
  Within the range of 7,. 0 to 10.0
            at all times
Ingot Conveyer Casting Contact Cooling  (When Chlorine
    Demagging Wet Air Pollution Control is; Practiced "On-Site)
Pollutant or
Pollutant property
Maximum for
any one day
  Maximum for
monthly average
              Metric Units - mg/kg of aluminum cast
        English Units - Ibs/million Ibs of aluminum cast
 Cadmium
*Lead
*Zinc
*Aluminum
*Ammonia (as N)
*Oil and Grease
*TSS
*pH

*Regulated Pollutant
     0.000                  0.000
     0.000                  0.000
     0.000                  0.000
     0.000                  0.000
     0.000                  0.000
     0.000                  0.000
     0.000                  0.000
  Within the range of 7.0 to 10.0
            at all times
                               1004

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          SECONDARY ALUMINUM SUBCATEGORY
               SECT - XI
                      TABLE XI-2  Continued)

           NSPS FOR THE SECONDARY ALUMINUM SUBCATEGORY
Stationary Casting Contact Cooling
Pollutant or
Pollutant property
Maximum for
any one day
  Maximum for
monthly average
              Metric Units - mg/kg of aluminum cast
        English Units - Ibs/million Ibs of aluminum cast
 Cadmium
*Lead
*Zinc
*Aluminum
*Ammonia (as N)
*Oil and Grease
*TSS
*pH

*Regulated Pollutant
     0.000                  0.000
     0.000                  0.000
     0.000                  0.000
     0.000                  0.000
     0.000                  0.000
     0.000                  0.000
     0.000                  0.000
  Within the range of 7.0 to 10.0
            at all times
Shot Casting Contact Cooling

Pollutant or
Pollutant property
Maximum  for
any one  day
  Maximum  for
monthly  average
              Metric Units - mg/kg of aluminum cast
        English Units - Ibs/million Ibs of aluminum cast
 Cadmium
 *Lead
 *Zinc
 *Aluminum
 *Ammonia  (as N)
 *Oil and Grease
 *TSS
 *pH

 *Regulated  Pollutant
      0.000                   0.000
      0.000                   0.000
      0.000                   0.000
      0.000                   0.000
      0.000                   0.000
      0.000                   0.000
      0.000                   0.000
   Within the range of  7.0  to 10.0
             at all times
                                1005

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SECONDARY ALUMINUM SUBCATEGORY    SECT - XI
     THIS PAGE  INTENTIONALLY  LEFT BLANK
                   1006

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          SECONDARY ALUMINUM  SUBCATEGORY     SECT  -XII
                           SECTION XII

                      PRETREATMENT STANDARDS
Section 307 (b)  of the Act requires EPA to promulgate pretreatment
Standards  for   existing sources (PSES),   which must be  achieved
wi?hin three years of promulgation.  PSES are designed to prevent
    discharge of pollutants which pass through,  interfere  with,
promulgated in 1974, is based on oil skimming, pH adjustment, and
ammonia air stripping technology.

Section 307 (c) of the Act requires EPA to promulgate pretreatment
standards  for  new  sources  (PSNS) at the  same  time  that  it
promulgates  NSpS    New indirect discharge facilities,  like new
di?ect discharge facilities,  have the opportunity to incorporate
?he Ces? amiable demonstrated  technologies  J^f n\r*a^
chanaes     in-plant   controls,    and   end-of-pipe   treatment
technologies^  and to use plant  site selection to ensure adequate
treatment  system installation.   The existing PSNS is  based  on
lime   precipitation  and   sedimentation  with   in-process   flow
reduction.

Pr^n-Pat-ment   standards  for  existing and new sources are   to  be
?echno?ogy  based and analogous  to  the best available   technology
and  the best  demonstrated technology,  respectively,  f or _ removal
of   toxic  pollutants.   For  this reason,  EPA is  modifying  the
existing PSES and PSNS.

This section  describes  the  control  technology for pretreatment of
process  wastewaters  from existing  sources and new  sources in  the
 secondary  aluminum  subcategory.     Pretreatm ent   standa ™  *°F
 regulated  pollutants  are presented  based on  the  described  control
 technology.

 TECHNICAL  APPROACH  TO PRETREATMENT

 Before  promulgating  pretreatment standards,   the  Agency examines
 whether  the  pollutants discharged by the subcategory pass  through
 the  POTW  o?  interfere with the POTW operation  or  its   chosen



 wi?h 9theY percentage removed by .direct dischargers ^plying  the
 best available technology economically achievable.    A  pollutant
 is  delmed to pass through the POTW when the  average  percentage
 removed   nationwide  by  well-operated  POTW  meeting  secondary
 treatment  refinements  is  less than the percentage   removed  by
 direc? Dischargers  complying  with  BAT  effluent    lotions
 guidelines for that pollutant.  (see generally, 46 PR  at 9415 16,
                                1007

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            SECONDARY ALUMINUM SUBCATEGORY     SECT  -XII
  January  28,  1981).

  This   definition    of  pass   through   satisfies  two   competing
  objectives   set  by  Congress:    (1)  that standards  for  indirect
  dischargers  be  equivalent  to  standards for  direct  dischargers,
  while  at  the same  time,   (2) that  the treatment capability  and
  performance  of  the  POTW be recognized and taken into account  in
  regulating the discharge of pollutants from indirect dischargers
  The  Agency  compares percentage  removal rather than the  mass  or
  concentration  of pollutants discharged because the latter  would
  S?*L fc|ke  into  account the mass of pollutants discharged to  the
  POTW  from   non-industrial  sources  nor  the  dilution  of   the
  pollutants   in   the POTW effluent to lower concentrations due  to
  tne addition of  large amounts of non-industrial wastewater.

 PRETREATMENT STANDARDS FOR EXISTING AND NEW SOURCES

 Options  for pretreatment of wastewaters from both  existing  and
 new  sources are based on increasing the effectiveness of end-of-
     «£re*  e?fc technologies.  All in-plant changes and applicable
    -of-pipe treatment processes have been discussed previously in
 Sections  X and XI.   The options for PSNS and PSES,  therefore/are
 the same  as_the BAT options discussed in Section X.   Although oil
 and grease is a conventional pollutant  compatible with  treatment
            £ P°TW'   Oil Skimmin9  ^ needed for  the  PSNS  trlatmSnt
             u ensure Proper removal.    Oil  and  grease   interferes
  ™<      - Chemi5ai  Edition  and mixing  required   for   chemical
 precipitation and treatment.
A  description  of   each   option  is   presented   in   Section
Treatment  technology options  for the  PSES  and  PSNS are:

OPTION A
                                                        X,
     o  Preliminary  treatment with oil  skimming  (where  required)
     o  Preliminary  treatment of dross  washing wastewater with
        ammonia steam stripping
     o  Preliminary  treatment of delacquering wet air pollution
        control wastewater with activated carbon adsorption
     o  In-process flow reduction of casting contact cooling
        water and scrubber liquor resulting from scrap drying and
        delacquering wet air pollution  control       '
     o  Chemical precipitation and sedimentation
OPTION C
     o  Preliminary treatment with oil skimming (wf ere required)
     o  Preliminary treatment of dross washing wastfewater with
        ammonia steam stripping                   :
                                                   ir pollution
Preliminary treatment of delacquering wet a
control wastewater with activated carbon   :
In-process flow reduction of casting contact cooling
water and scrubber liquor resulting from scrap drying and
delacquering wet air pollution control
Chemical precipitation and sedimentation   ,\
                               1008

-------
          SECONDARY ALUMINUM SUBCATEGORY
SECT -XII
     o  Multimedia filtration

INDUSTRY COST AND POLLUTANT REMOVAL ESTIMATES

The  industry  cost and environmental benefits of each  treatment
option were used to determine the most cost-effective option. The
methodology  applied in calculating pollutant  removal  estimates
and plant compliance costs is discussed in Section X.          ,j
                                                               it
Table  XII-1  (page 1011) shows the estimated  pollutant  removal
estimates  for  indirect  dischargers.    Compliance  costs   a|re
presented in Table VIII-2, (page 971).                         f

PSES AND PSNS OPTION SELECTION

The  technology  basis  for  the promulgated  PSES  and  PSNS  Us
identical  to  BAT  (Option  C)  and  NSPS,   respectively.   Tiae
treatment   scheme   consists  of  in-process    flow   reductioi ,
preliminary  treatment  with ammonia  steam  stripping,  activated
carbon adsorption, and oil skimming  (where required), followed by
lime precipitation,  sedimentation, and filtration.  EPA knows of
no demonstrated technology that provides more efficient pollutant
removal  than BAT  technology.   No additional flow  reduction  for
new  sources  is feasible because the only other available   flow
reduction   technology,   reverse  osmosis   (Option F)  is    not
adequately  demonstrated nor is  it clearly transferable for   this
subcategory.  Just as in the  BAT effluent   limitations,   at-the-
source monitoring  and compliance  is  required  for total  phenolics
in delacquering wet air  pollution control wastewater.

The   selected   option   for   PSES   increases   the    removal   of
approximately 11,300 kg/yr of  toxic  metals and  210  kg/yr of  total
phenolics   over  the estimated  raw discharge.    Estimated   removal
over  the   intermediate  option considered  is  11.6 kg/yr of  toxic
metals.  The  estimated capital cost  of  PSES  is  $2.3 million  (1982
dollars) and  the  annual  cost  is $1.4 million (1982  dollars).

REGULATED  POLLUTANT PARAMETERS

Pollutants  selected   for  regulation under   PSES  and  PSNS  are
 identical   to  those   selected  for   regulation  for  BAT.    The
 conventional   pollutants  oil  and grease,   TSS,  and PH  are  not
 limited   under  PSES   and  PSNS  because  they  are  effectively
 controlled  by POTW.    PSES and PSNS prevent the pass-through  of
 lead,  zinc, ammonia,  and total phenols.  The toxic pollutants are
 removed by well-operated POTW on an average of  53 percent (lead -
 49 percent, zinc - 65  percent, phenol - 96 percent, and ammonia -
 0 percent). Aluminum is not limited because in  its hydroxide form
 it  is   used  by POTW as a flocculant aid  in   the  settling  _and
 removal  of  suspended  solids.  As  such,  aluminum  in  limited
 quantities  does not pass through or interfere  with POTW;    rather
 it is a necessary aid to its operation.
                                1009

-------
           SECONDARY ALUMINUM SUBCATEGORY    SECT -XII


 PRETREATMENT STANDARDS

 In  proposing  PSES and PSNS,  the Agency considered  whether  to
 propose exclusively mass-based standards,  or to allow a POTW the
 alternative of concentration or mass-based standards.  Mass-based
 standards  ensure  that  limitations  are achieved  by  means  of
 pollutant removal rather than by dilution.  They are particularly
 important when a limitation is based upon flow reduction  because
 pollutant  limitations associated with the flow reduction  cannot
 be measured any way but as a reduction of mass discharged.   Mass-
 based standards,  however, are harder to implement because  a POTW
 faces  increased  difficulties in monitoring.    A POTW also  must
 develop  specific  limits  for  each  plant  based  on  the  unit
 operations   present  and  the  production  occurring   in    each
 operation.

 EPA  resolved  these competing considerations  by proposing   mass-
 based  standards  exclusively where  the PSES and  PSNS  treatment
 options include significant flow reductions or where  significant
 pollutant  removals   are attributable to flow   reductions.    Flow
 reduction over  current discharge rates was minimal  (0.2   percent)
 in the  secondary aluminum subcategory in the proposed, standards.
 For  secondary   aluminum,  EPA concluded that  the   proposed  PSES
 should   provide  alternative  mass-based  and  concentration-based
 standards.

 The  addition   of ingot  conveyer  casting,  however,   now   requires
 substantial   flow   reduction    for    the  secondary    aluminum
 subcategory.    Recycle of  ingot  conveyer  casting is  based  on  90
 percent   recycle   when demagging  scrubbers are not  used   and  100
 percent   reuse  in demagging air pollution  control when  scrubbers
 are   used.  It  is  now  estimated  the PSES  technology   will   reduce
 current   flows  by  25 percent.  Consequently,  concentration-based
 standards are not  promulgated for this  subcategory  to ensure that
 flow  reduction  is  achieved.

 The PSES discharge flows are identical  to  the BAT discharge flows
 for  all  processes.   These discharge  flows are listed in  Table
 XII-2, (page 1012) As  shown in Table XII-3  (page 1014), the  PSNS
 discharge  flows  are  identical to the NSPS flows.  The  mass  of
pollutant  allowed  to  be  discharged per  mass  of  product  is
 calculated by multiplying the achievable treatment  concentration
 (mg/1) by the normalized wastewater discharge flow (1/kkg).   PSES
and  PSNS  are shown in Tables XII-4 and XII-5, (pages  1016  and
1020) respectively.
                               1010

-------
                     SECONDARY  ALUMINUM  SUBCATEGORY
                                                             SECT  -  XII
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-------
           SECONDARY ALUMINUM SUBCATEGORY
                SECT -XII
                            TABLE XI1-4

            PSES FOR THE SECONDARY ALUMINUM SUBCATEGORY
 Scrap Drying Wet Air Pollution Control
 Pollutant or
 Pollutant property
 Maximum for
 any one day
   Maximum for
 monthly average
           Metric Units - mg/kg of aluminum scrap dried
      English Units - Ibs/million Ibs of aluminum scrcip dried
  Cadmium                          0.000
 *Lead                             0.000
 *Zinc                             0.000
 *Ammonia (as  N)                    0.000

 *Regulated  Pollutant
                             0.000
                             0.000
                             0.000
                             0.000
 Scrap  Screening  and Milling

 Pollutant or                 Maximum  for
 Pollutant property	any one  day	
 Metric Units - mg/kg of aluminum delacquered
 English Units -Ibs/million Ibs of aluminum scrap screened  & milled
                       Maximum  for
                     monthly average
 Cadmium
*Lead
*Zinc
*Ammonia  (as N)

*Regulated Pollutant
     0.000
     0.000
     0.000
     0.000
       0.000
       0.000
       0.000
       0.000
Dross Washing

Pollutant or
Pollutant property
Maximum for
any one day
  Maximum for
monthly average
              Metric Units - mg/kg of dross washed
         English,Units - Ibs/million Ibs of dross washed
 Cadmium
*Lead
*Zinc
*Ammonia (as N)

*Regulated Pollutant
     2.174
     3.043
    11.090
  1449.000
       0.869
       1.413
       4.565
     636.900
                               1016

-------
          SECONDARY ALUMINUM SUBCATEGORY
                 SECT -XII
                      TABLE XI1-4 (Continued)

           PSES FOR THE SECONDARY ALUMINUM SUBCATEGORY


Demagging Wet Air Pollution Control
Pollutant or
Pollutant property
  Maximum for            Maximum for
  any one day	monthly average
mg/kg of aluminum demagged
            Metric Units   ..._,  ^
      English Units - Ibs/million Ibs of aluminum demagged
 Cadmium
*Lead
*Zinc
*Ammonia (as N)

*Regulated Pollutant
       0.139
       0.195
       0.711
      92.910
       0.056
       0.091
       0.293
      40.850
Delacquering Wet Air Pollution Control

Pollutant or                 Maximum for            Maximum for
Pollutant property	any one day 	monthly average
          Metric Units - mg/kg of aluminum delacquered
     English Units - Ibs/million Ibs of aluminum delacquered
 Cadmium                          0.016
*Lead                             0.022
*Zinc                             0.082
*Ammonia  (as N)                  10.670
*Total Phenols(4-AAP) **          0.001

*Regulated Pollutant
**At the  source
                              0.006
                              0.010
                              0.034
                              4.688
Direct Chill Casting Contact Cooling
Pollutant or
Pollutant property
   Maximum for
   any  one day
  Maximum for
monthly average
          Metric Units - mg/kg  of  aluminum  delacquered
      English Units  -  Ibs/million Ibs  of  aluminum delacquered
  Cadmium
 *Lead
 *Zinc
 *Ammonia  (as  N)

 *Regulated Pollutant
        0.266
        0.372
        1.356
      177.200
       0.106
       0.173
       0.558
      77.880
                                1017

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           SECONDARY ALUMINUM SUBCATEGORY
               SECT -XII
                       TABLE XII-4  (Continued)

            PSES  FOR THE SECONDARY  ALUMINUM  SUBCATEGORY
 Ingot  Conveyer  Casting  Contact  Cooling  (When  Chlorine
     Demagging Wet  Air Pollution Control  is Not  Practiced On-Site)
 Pollutant  or
 Pollutant  property
Maximum for
any one day
  Maximum for
monthly average
          Metric Units  - mg/kg  of aluminum cast
     English Units  -  Ibs/million Ibs of aluminum  cast
  Cadmium
 *Lead
 *Zinc
 *Ammonia  (as N)

 *Regulated Pollutant
     0.009
     0.012
     0.044
     5.732
       0.003
       0.006
       0.018
       2.520
Ingot Conveyer Casting Contact Cooling  (When Chlorine
    Demagging Wet Air Pollution Control is Practiced On-Site)
Pollutant or
Pollutant property
Maximum for
any one day
  Maximum for
monthly average
              Metric Units - mg/kg of aluminum cast
        English Units - Ibs/million Ibs of aluminum cast

 Cadmium                          0.000                  0.000
*Lead                             0.000                  0.000
*Zinc                             0.000                  0.000
*Ammonia (as N)                   0.000                  0.000

*Regulated Pollutant
Stationary Casting Contact Cooling

Pollutant or.                 Maximum for            Maximum for
Pollutant property	any one day	monthly average
              Metric Units - mg/kg of aluminum cast
        English Units - Ibs/million Ibs of aluminum cast
 Cadmium
*Lead
*Zinc
*Ammonia (as N)

*Regulated Pollutant
     0.000
     0.000
     0.000
     0.000
       0.000
       0.000
       0.000
       0.000
                               1018

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          SECONDARY ALUMINUM SUBCATEGORY
               SECT -XII

                      TABLE XII-4 (Continued)

           PSES FOR THE SECONDARY ALUMINUM SUBCATEGORY
Shot Casting Contact Cooling

Pollutant or
Pollutant property
Maximum for
any one day
  Maximum for
monthly average
              Metric Units - mg/kg of aluminum cast
        English Units - Ibs/million Ibs of aluminum cast
 Cadmium
*Lead
*Zinc
*Ammonia (as N)

*Regulated Pollutant
     0.000
     0.000
     0.000
     0.000
       0.000
       0.000
       0.000
       0.000
                                1019

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           SECONDARY ALUMINUM SUBCATEGORY
                SECT -XII
                            TABLE XII-5

            PSNS FOR THE SECONDARY ALUMINUM SUBCATEGORY


 Scrap Drying Wet Air Pollution Control

 Pollutant or                 Maximum for            Maximum for
 Pollutant property	any one day	monthly average
           Metric Units - mg/kg of aluminum scrap dried
      English Units - Ibs/million Ibs of aluminum scrap dried
  Cadmium
 *Lead
 *Zinc
 *Ammonia (as N)

 *Regulated Pollutant
      0.000
      0.000
      0.000
      0.000
        0.000
        0.000
        0.000
        0.000
 Scrap  Screening  and Milling

 Pollutant  or                 Maximum  for            Maximum  for
 Pollutant  property	any one  day	monthly average
    Metric^Units - mg/kg of aluminum  scrap  screened & milled
 English Units-lbs/million  Ibs of aluminum scrap screened & milled
 Cadmium
*Lead
*Zinc
*Ammonia  (as N)

*Regulated Pollutant
     0.000
     0.000
     0.000
     0.000
       0.000
       0.000
       0.000
       0.000
Dross Washing

Pollutant or
Pollutant property
Maximum for
any one day
  Maximum for
monthly average
              Metric Units - mg/kg of dross washed
         English Units - Ibs/million Ibs of dross washed
 Cadmium
*Lead
*Zinc
*Ammonia (as N)

*Regulated Pollutant
     0.000
     0.000
     0.000
     0.000
       0.000
       0.000
       0.000
       0.000
                               1020

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          SECONDARY ALUMINUM SUBCATEGORY
               SECT  -XII
                      TABLE XII-5 (Continued)

           PSNS FOR THE SECONDARY ALUMINUM SUBCATEGORY


Demagging Wet Air Pollution Control

Pollutant or                 Maximum for            Maximum for
Pollutant property	any one day	monthly average
           Metric Units - mg/kg of aluminum demagged
      English Units - Ibs/million Ibs of aluminum demagged
 Cadmium
*Lead
*Zinc
*Ammonia (as N)

*Regulated Pollutant
     0.139
     0.195
     0.711
    92.910
       0.056
       0.091
       0.293
      40.850
Delacquering Wet Air Pollution Control
Pollutant or
Pollutant property
Maximum for
any one day
  Maximum for
monthly average
          Metric Units - mg/kg of aluminum delacguered
     English Units - Ibs/million Ibs of aluminum delacquered
 Cadmium                          0.016
*Lead                             0.022
*Zinc                             0.082
*Ammonia  (as N)                  10.670
*Total Phenols(4-AAP) **          0.001

*Regulated Pollutant
**At the  source
                            0.006
                            0.010
                            0.034
                            4.688
Direct Chill Casting Contact Cooling
 Pollutant or
 Pollutant property
Maximum for
any one day
  Maximum for
monthly average
              Metric Units  - mg/kg  of  aluminum  cast
         English Units  -  Ibs/million Ibs  of  aluminum  cast
  Cadmium
 *Lead
 *Zinc
 *Ammonia (as  N)

 *Regulated  Pollutant
     0.266
     0.372
     1.356
    177.200
       0.106
       0.173
       0.588
       77.880
                                1021

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           SECONDARY ALUMINUM SUBCATEGORY
                SECT  -XII
                       TABLE XII-5  (Continued)

            PSNS  FOR THE SECONDARY  ALUMINUM SUBCATEGORY
 Ingot  Conveyer  Casting  Contact  Cooling  (When Chlorine
     Demagging Wet Air Pollution is  Not  Practiced On-Site)
 Pollutant  or
 Pollutant  property
Maximum  for
any one  day
  Maximum  for
monthly  average
              Metric Units  - mg/kg of aluminum cast
        English Units -  Ibs/million  Ibs of aluminum cast
 Cadmium
 *Lead
 *Zinc
 *Ammonia  (as N)

 *Regulated Pollutant
     0.009
     0.012
     0.044
     5.732
        0.003
        0.006
        0.018
        2.520
Ingot Conveyer Casting Contact Cooling  (When Chlorine
    Demagging Wet Air Pollution Control is Practiced On-Site)
Pollutant or
Pollutant property
Maximum for
any one day
  Maximum for
monthly average
              Metric Units - mg/kg of aluminum cast
        English Units - Ibs/million Ibs of aluminum cast
 Cadmium                          0.000
*Lead                             0.000
*Zinc                             0.000
*Ammonia (as N)                   0.000

*Regulated Pollutant
                            0.000
                            0.000
                            0.000
                            0.000
Stationary Casting Contact Cooling
Pollutant or
Pollutant property
Maximum for
any one day
  Maximum for
monthly average
              Metric Units - mg/kg of aluminum cast
        English Units - Ibs/million Ibs of aluminum cast
 Cadmium
*Lead
*Zinc
*Anunonia (as N)

*Regulated Pollutant
     0.000
     0.000
     0.000
     0.000
       0.000
       0.000
       0.000
       0.000
                               1022

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          SECONDARY ALUMINUM SUBCATEGORY
               SECT -XII

                      TABLE XII-5 (Continued)

           PSNS FOR THE SECONDARY ALUMINUM SUBCATEGORY
Shot Casting Contact Cooling

Pollutant or
Pollutant property
Maximum for
any one day
  Maximum for
monthly average
          Metric Units - mg/kg of aluminum scrap dried
     English Units - Ibs/million Ibs of aluminum scrap dried
 Cadmium
*Lead
*Zinc
*Ammonia (as N)

*Regulated Pollutant
     0.000
     0.000
     0.000
     0.000
       0.000
       0.000
       0.000
       0.000
                               1023

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SECONDARY ALUMINUM SUBCATEGORY    SECT -XII
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                    1024

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         SECONDARY ALUMINUM SUBCATEGORY
SECT - XIII
                           SECTION XIII

          BEST CONVENTIONAL POLLUTANT CONTROL TECHNOLOGY
EPA  is  not  promulgating best  conventional  pollutant  control
technology  (BCT) for the secondary aluminum subcategory at  this
time.
                               1025

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SECONDARY ALUMINUM SUBCATEGORY    SECT - XIII
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                     1026

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