EPA 450/2-74-020b
October 1974
        BACKGROUND INFORMATION
   FOR STANDARDS OF  PERFORMANCE:
      PRIMARY  ALUMINUM INDUSTRY
    VOLUME 2:   TEST  DATA SUMMARY

         U.S. ENVIRONMENTAL PROTECTION AGENCY
           Office of Air aud Waste Management
         Office of Air Quality Planning and Standards
         Research Trianele Park. North Carolina 27711

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                                  EPA-450/2-74-020b
     BACKGROUND INFORMATION
FOR  STANDARDS  OF PERFORMANCE:
   PRIMARY ALUMINUM  INDUSTRY
  VOLUME  2:  TEST DATA  SUMMARY
          Emission Standards and Engineering Division
         U.S. ENVIRONMENTAL PROTECTION AGENCY
            Office of Air and Waste Management
          Office of Air Quality Planning and Standards
         Research Triangle Park, North Carolina 27711

                    October 1974

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This report is issued by the Environmental Protection Agency to report
technical data of interest to a limited number of readers.  Copies are
available free of charge to Federal employees, current contractors and
grantees, and nonprofit organizations - as supplies permit - from the Air
Pollution Technical Information Center, Environmental Protection Agency,
Research Triangle Park, North Carolina 27711; or,  for a fee, from the
National Technical Information Service, 5285 Port Royal Road, Springfield,
Virginia 22161.
                  Publication No.  EPA-450/2-74- 020b
                                  II

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                                  CONTENTS
Section
INTRODUCTION  	
FLUORIDE TEST RESULTS   .  .
FACILITIES .	•  .  ,
SUMMARY OF RESULTS 	
REFERENCES .  .	
TECHNICAL REPORT DATA SHEET.
Page
  1
  2
  2
 n
 46
 48

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                              PRIMARY ALUMINUM INDUSTRY
 INTRODUCTION                                               ;
    |                                        .                I
    j  This document presents a summary of source tests and visible emission
 measurements cited in "Technical Report:  An Investigation of the Best Systems
 of Emission Reduction for the Primary Aluminum Industry."  It is concerned
 principally with tests for fluorides and visible emissions, but also describes
 the facilities  from which data have been obtained,  their operating conditions,
 and:characteristics of exhaust gas  streams.
    l                       .               •                  i

      Facilities  are identified by the  same coding used  in the Technical  Report
    i                                             .                           '
 (excjept  as  noted in the  facility descriptions).  For  example, Table  1  (Facility A,)
 summarizes  results  of EPA's May  1972 measurements of  primary  emissions from Plant
    i                                                        i
 A.  jThese same results are also  plotted  in Figure 11  of  the Technical  Report
 identified as Plant A-,.

    j Many of the tests summarized herein were conducted  us i rig EPA Method 13
for [fluorides.  This method will be proposed in the Federal Register at the
time)of proposal of standards of performance for new or substantially modified
primary aluminum plants.                                     !

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Fluoride Test Results
     A program was undertaken by EPA to evaluate the best control  techniques
available for controlling fluoride emissions from primary aluminum plants.
The data obtained serves as input to development of standards of performance
for primary aluminum plants being proposed under section 111  of the Clean
Air Act of 1970.
     Preliminary investigation revealed the locations of a number, of reportedly
well controlled plants.  Eight of these were visited to obtain further information
on the process and air pollution control equipment.  Six plants were selected
for emission  tests.  These plants represented all three types of reduction cells
and a variety of  air pollution control systems.  Two of these plants were later
retested.  Two other plants were inspected  in Europe, and emission data was
furnished  by  their owners.  Additional data was  obtained from American aluminum
companies  and from state air  pollution control  agencies.
      Figures  1,  2, and 3 present a  visual  comparison of the  data.
 Facilities
      Potroom Facilities
      A.  Plant A is a vertical stud Soderberg plant with a production capacity
    -•  -  ofl88sOOO;*t6ns"p^Fye&r°6f aluminum.  The plant'has two pot lines with
          150 cells (pots) per line housed in four,potrooms.  The primary emission
          control system consisted of a "bubbler" scrubber followed by a wet

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    electrostatic precipitator.  The secondary system consisted of a
    spray screen scrubber at the roof monitors.  The primary emissions
    were tested twice by an EPA contractor (tests'A. and A.) using EPA
    Method 13 for fluorides.  Additional primary emission data, results
    of emission measurements performed by the company, were furnished
    by a state agency (A3).  Secondary emissions were tested by EPA
    contractors three times.  Jests A, and A  were performed in
                                     I      £
    conjunction with the.respective primary emission tests A. and A.,
    while test A was performed on a separate occasion.  Additional
    secondary emission data:from company tests was provided by a state
    agency (A3) and by the company itself (A ).   EPA Method 13 was used
    for tests A and A,, of secondary emissions.  Company test methods
    were used for the other secondary emission tests.
B.  This is a horizontal stud Soderberg plant with a production capacity
    of 190,000 tons per year of aluminum.  The newer portion of the plant
    tested consisted of three potlines with 168 ce;lls  per line housed in
    six potrooms.   The primary emission control  system used at this plant
    consisted of a venturi  scrubber using a caustic solution, so that
                                                 I
    the fluoride can be recovered,  followed by a wet electrostatic
    precipitator:   The plant did  not use a control-system fon.secondary
    emissions.   Primary and  secondary emissions  were both tested at this
    plant  by  an  EPA contractor  using EPA Method  13  (tests designated  B).
    Additional data on primary  and  secondary  emissions  (designated B,)
    were provided by the company.   The  test method  used  by  the  company
    is  not  known.

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C.  This is a prebake plant with a production capacity of 175,000 tons
    per year of aluminum.  Aluminum is produced from five pot! ines with
    about 156 cells per line.  The primary emission control  system used
    on the potroom tested was a fluid bed dry scrubber Using alumina
    as the scrubbing medium and a baghouse as the collector.  The plant
    did not use a control system for secondary emissions.  Primary and
    secondary emissions were both tested at this plant using EPA Method
    13.   "  -'  -  ••  '• '-  "'•  "" '? ........... ;—»•--•-; .......... .- •<;  -M.+ ««••'*•

D.  This is a prebake plant with a production capacity of about 120,000
    tons per year of aluminum.  Aluminum is produced from two pot! ines
                                                                       *
    containing 124 cells per line.  The potlines are housed in four
    potrooms.  The primary emission control system used on the potroom
    tested was a fluid bed dry scrubber using alumina as the scrubbing
    medium and a baghouse as the collector.  The plant did not use a
    control system for secondary emissions.  Primary emissions were
    tested twice by EPA  (tests designated D and D^) and secondary.
    emissions were tested once.  EPA Method 13 was used to conduct all
    tests.  Visible emission data for both primary and secondary emissions
    were  obtained by EPA and contractor personnel using EPA Method 9 on
    another occasion.
E.  These data are not specific tosawy dfle^1ari%-J but 'are primary and
    secondary emission data provided by the owner of Facilities C and D.
    Tests were conducted. using the company's own test method.— r-   --

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 F.  This  is a'European vertical  stud  Soderberg  plant which  produces
    about 25,000 metric tons of  aluminum per year, j Aluminum  is
    produced from one potroom containing 88 cells.  The  primary
    emission control system consists  of cyclones  in series  with
    fluid bed dry scrubbers using alumina as the  scrubbing  medium
    and baghouses as collectors.  Secondary emissions are controlled
    by scrubbing towers using sea water as the  scrubbing medium.
    Gas from the primary control system is also routed through the  '"
    secondary system scrubbers.  Both primary and secondary control
    systems were tested by the owner of the plant.  Only primary
                                                   r
    emission data are utilized.  Test methods are uiiknown.
G.
H.
This is a European plant using prebake  cells which  produces  about
80,000 metric tons of aluminum per year from 216  cells.  A dry
                                                *
primary emission control system is used.  There is  no secondary
emission control system.  Both primary  and secondary emission
data were provided by the owner.  Test  methods are  unknown.
(Secondary emission data for this facility is coded as "Plant F"
in Figure 12 of the Technical Report.)

This plant uses prebake cells and produces 265,000  tons of aluminum
per year.  The primary control system is an injected alumina dry
                ;                      '         I.
scrubber.  Secondary control;is by^aopowered concurrent spray scrubber.
Both primary and secondary emission data was submitted by a state air
pollution control agency.  The test method is unknown.  (Secondary
emission data for this facility is coded as "Plant G" in Figure 12
                               - .      .         i.
of the Technical Report.)

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Anode Plants
A.  This plant started production late in 1970 and has  a production
    capacity of about 75,000 tons per year of anodes.   Anodes  are
    produced by crushing and sizing the raw material,  coke,  and mixing
    it with pitch (tar).  The anode blocks are produced in a hydraulic
    unit which presses the coke-tar mixture into blocks.  The blocks
    are then placed in the anode furnace to bake for about 30 days
    at 1100-1200°C.  The emissions from the anode bakTfuWace are
    collected in two parallel 54-inch ducts which are  each connected
    to a water spray tower and electrostatic precipitators in series.
    The water spray towers condense much of the tar in the gases  and
    closely controls the temperature of the gases entering the electro-
    static precipitator.  After the spray towers and precipitators,
    the gas stream!is combined and is discharged from a 2.7 meter
    (nine-foot) diameter, 53 meter (175 feet) high stack.  This facility
    was tested by EPA using Method 13 for fluorides.  Visible emission
    data were obtained using EPA Method 9 by EPA and contractor
    personnel on a separate occasion.
B.  This plant started production of anodes in 1971 with a production
    capacity of about 230,000 tons per year of anodes.  Anodes are
    produced by crushing and sizing the raw material, coke, which
    is then mixed with pitch (tar).  The anode blocks are produced in
    a vibrator unit which!compacts the coke-tar mixture into blocks.
    The blocks are then placed in the anode furnace to bake for about

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30 days at n50-1200°C.  The emissions from the anode furnace are
                                               i

collected in two 54-inch ducts which join together at a water spray


conditioning chamber.  The chamber condenses much of the tar and
                                               i.

provides close temperature control of the gas stream entering the
                                               'l

electrostatic precipitator.  The gas discharges through a 30 meter
                                        • '      u

(100 foot) stack.  This facility was tested by EPA contractors


using EPA Method 13.                                  •

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0.80
0.60
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ee
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VSS VSS VSS HSS HSS PB PB PB PB VSS PB PB
BS-P BS-P BS-P ST-P ST-P FBDS FBDS FBDS FBDS FBDS IADS IADS -'
Figure 1.  Primary emis'siorts from the primary aluminum.reduction industry.

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| CONTROL    SS     SS     SS    SS    SS    NC    NC   NC    NC   NC    NC    PCS
EQUIPMENT          ••.,','.


|             Figure 2.  Secondary emissions from the primary aluminum reduction industry.
•J.13

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EQUIPMENT ELECTROSTATIC PRECIPITATORS
                 Figure 3. Carbon anode bake plant emissions.
10

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                  ...      •,:..,,.,. .Table 1          •    -




                   FACILITY - AI   (Primary Outlet1- Fluorides)



                             Summary of Results
Run. number
Date
Test Time-minutes
Production rate - TPH
Stack Ef flue'nt ,
Flow rate - DSCFM
Flow rate '"- DSCF/ton
Temperature - °F
Water- vapor - Vol. °L
C02 - Vol. - % dry
02 - Vol. % dry
CO - Vol. % dry
Visible Emissions - % opacity
Fluorides
.Soluble ' • • '
gr/DSCF - ' •
. gr/ACF
Ib/hr • .' ,
Ib/ton of product
Total Fluorides
• gr/DSCF ' r
gr/ACF
Ib/hr .-.••=•••?'
Ib/ton of product
.1
5/8/72
288
0.512

5758.0
663,000
52.0
2.38 '
6.0
15.5
0.0
5%

0.000145
0.000147
., , 0.00715
0.0140

0.000167
O.J5QQ170
0.00825
Oi-01-61
2 .
5/9/72
288
0.512

5999.8
586,000
.52.2
2.65
6.0
., .15.5
' I
0.0 \
5% ; •

0.000118
0.000120
. i>-. 0.00516
a o.oioi

!•
'o'. 000118
0.000120
0.00516
0.0101
3 '-'.
5/9/72
288 \
Q.512 }
i
5114.7 :
. 588,000
51.7 ;•
2.60 ,
6.0
15.5 •
, 0.0
5% '
. ' j-
0.000124'
0. 000125*.
0.00535
0.0104

• ' ' Jilt
0.000124
0.000125
0.00535
0.0104
Average

288
, 0.512
*"• • f*
5324. 2
612,333
52.0
2.51 ;';
6.0
15.5. ;
0.0
.5%

0.000129
0.000131
.0.00587
6.0115
-,-.--.-/
^q.;ur.^
'0.000136
0. 000138
0.000625
0.0122
Reference 1.
                                                                           11

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                                  Table' 2  >





                      FACILITY - A£  (Primary Outlet - Fluorides)



                                Summary of Results
Run number

Date
Test Tirne-minutes
Production rate - TPH
Stack Effluent
Flow rate - DSCFM
Flow rate - DSCF/ton
Temperature - °F
Water vapor - Vol. %
C02 - Vol. 7. dry
02 - Vol. % dry
CO - Vol. 7. dry
Visible Emissions - % opacity
Fluorides
Soluble
gr/DSCF
gr/ACF
Ib/hr
Ib/ton of product "
Total Fluorides
gr/DSCF
gr/ACF
Ib/hr
Ib/ton of product
1
ir\/o o/~7o
10/2-3/72
1442
0.516
•""*
3929
7614
,81
3.3
"6.0
15.5
0.0
0-5


0.000084
0.000080
0.0028
0.0060

0.000087
0.000082
0.0030
0.0006
2
/
10/3-4/72
• 1440
0.516
«•'•*- •*
4705
9188
81
3.2
6.0
15.5
0.0
0-5


: 0.00016
0.00015
0.0068
0 1*013

0.00016
0.00016
0.0069
0.013
3

10/4-5/72-
1080
0.516
<- . -i'UJ
5187
10052
80
3.5
6.0
15.5
0.0
0-5
. .. ,-;: '.

0.00027
0.00026
0.0128
6.025

0.00029
0.00028
0.014
0.027
, Ayerage

'•-• • "'
•1321
A5l.fr

-. , ,4607
'"8928:
; si •
-.. ;3,3.,, .
'6.'b:1
15,5
r;;o?b^-
" 1-^';
; /, ' -;_;$ : \ ; "
-, . -,;', 3 rf,:r-
0/00017
0.00016
0.0075
'"" 0/015

0.00018
0.00017
0.0079
olol6'"
12
    Reference 2.

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                               Table 3
                FACILITY A3  CPn'mary Outlet-Fluorides)
                          Summary of Results.
                       1
                    3/9/72
Run Number
Date
Test Time-miriutes
Production rate - TPH  —
Stack Eff1uent
   Flow rate - DSCFM   —
   Flow rate - DSCF/
               ton
   Temperature - °F   —
   Water vapor - Vol.% ~
   C02V Vol.% dry
   02 - Vol.% dry
   CO  - Vol.% dry
Visible Emissions -
   % opacity
Fluorides
   Soluble
     gr/DSCF
     gr/ACF
     Ib'/hr
     Ib/ton of product —
   Total Fluorides
    . gr/DSCF
     gr/ACF
    2         3         41         5
 3/14/72   3/15/72   3/16/72   3/17/72
   Average
                    0.000195  0.000236  0.-000268  0.000302  0.000385  OV000277
     Ib/ton of
        product
      CJ.0,0
                    0.020
 0:023
r.«>.,-.>
0.0275.    0.030
,0.028
Reference 3.
                                                                              13

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                                  Table  4


                    FACILITY - A  (Secondary Outlet - Fluorides)

                              Summary of Results
i
11/8/71
180
0.'256
2
11/9/71
180
0.256
3
11/9/71
180
0.256
                                                                   Average



                                                                    180

                                                                    0.256
                                  139,200     139,200    139,200    139,200

                                32,630,000  32,630,000  32,630,000*32,630,000
14
        Run number

        Date

        Test Time-minutes

        Production rate - TPH

        Stack Effluent

          Flow rate - DSCFM

          Flow rate - DSCF/ton

          Temperature - °F

          Water vapor - Vol.  %

          C02 - Vol.  % dry

          02  - Vol.  % dry

          CO  - Vol.  % dry

        Visible Emissions - % opacity

        Fluorides

         .Soluble

            gr/DSCF

            gr/ACF

            Ib/hr

            Ib/ton of product

       Total Fluorides

            gr/DSCF

            gr/ACF

            Ib/hr

            Ib/ton of product
* Sample not consistent with normal range, probable picked up
  particulate F during sample handling.   Probable average
  shown in parenthesis.
50
1.337
0.0
20.5
0.02
5-10%
0.00014 '
0.00014,
0.168
0.66
0.00023
0.00023
0.273
1.07
50
1.006
0.0
20.6
0.03
5-10%
0.00043
0.00044
. 0. 512
2.00
0.00800
0.00810
9.52
37.20*
53
1.922
0.0
20.6
0.03
5-10%
0.00041
0.00041
0.485
1.89
0. 00049
0.00049
0.572
2.24
51
1.088
0.0
20.6
, .0.027 .
- . . i. *-*,'. •
5-10%
0.00033
0. 00033
. 0.388
i,, iGj.
1.52
0.00291
0. 00294
3.455 ,
26.26*
(1.65)

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                                 Table 5


                  FACILITY .-.  AI   (Siecondary Outlet - Fluorides)


                            Summary of Results
Run number


Date


Test Time-minutes


Production rate - TPH


Stack Effluent


  Flow rate - DSCFM  '
                         • -1

  Flow rate' - DSCF/ton


  Temperature - °F


  Water vapor - Vol. %


  C02 - Vol. % dry


  02  - Vol. % dry


  CO  - .Vol. % dry


Visible Emissions -  % opacity


Fluorides


  Soluble


    gr/DSCF


    gr/ACF


    Ib/hr


    Ib/ton of  product


Total  Flupride.s


    gr/BSGF


    gr/ACF


     Ib/hr


     Ib/ton of product






  Reference  1.
    1           2           3       Average



  5/8/72      5/9/72;     5/9/72



  300         300        280         293.3



  0.256       0.256      0.256       0.256




                    I       k   ' '  .  .  _

  251,970     251,970    251,970     '251,970



59,000,000  59,000,000  59,000,000   59,000,000
50
1.34 '
6.0
15.5
0.0
5-10%
60 j „'
1.40 i
6.0
i
15.5
0.0
5-10%
60
0.995
6.0
15.5
0.0
5-10%
63.3
1.24
6.0
15.5
0.0
5-10%
0.00084
0.000087
0.182
0.711
0. 000084
0.000087
0.182
0.711
0. 000122
0.000123
0.263
1.026
i
0.000126
0.000128
0.273 i
I
1.066
0.000065
0.000066
0.141"
0.551
o;oooow;
0.000077
0.165
0.643
0.000090
0.000092
•'"'• 0.195
0.762
-ifciTCi'
""T37000095
0". 000097
0.207 .
0.806
                                          15
                                      .foil.-:

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                                 Table q


                     FACILITY -  A2  (Secondary Outlet - Fluorides)


                               Summary of Results-
   Run number


   Date


   Test Time-minutes


   Production rate - TPH


   Stack Effluent


     Flow rate - DSCFM


     Flow rate - DSCF/tpn


     Temperature - °F    *


     Water vapor - Vol.  %


     C02 - Vol.  7. dry


     02  - Vol.  7. dry  ,


     CO  - Vol.  7. dry
                       A

   Visible Emissions - % opacity


   Fluorides


     Soluble


       gr/DSCF


       gr/ACF


       Ib/hr


       Ib/ton of product


  Total  Fluorides


       gr/DSCF  '


       gr/ACF


       Ib/hr


       Ib/ton of product



  Reference 2.
 10/2-3/72


   1440


   0.258






   253,000


59,000,000


   74


   2.0


   6.0


   15.5


   0.0


   0-5%
   2          3       Average


10/3-4/72   10/4-5/72
                          •v '  .


  1440       1440       1440



  0.258      0.258      0.258
            i •       ,'.': '...'•'.','.,, i*.





  255,100    261,000    256,700
                     > i .  •-• -• ,<-.,''. "


59,300,000, 61,100,000  59,800,000
  71


  1.9


  6.0


  15.5


  0.0


  0-57.
 64


 1.5


.6.0


 15.5


.0.0


 0-57o
70
1,8.
6.6


15-5
0.00.032
0.00031
0.703
2.73
0. 00035
0.00034
0.757
2.93
0.00017
0100016
0.363
i.4. ;'...,.•
0. 00017
0.00016
0.367
1.42
0.00020
0.00020
0.450
'^- -
0. 00021
0.00021
0.468
1.81
0.00023
0.00022
0.505
,,1,96
,0. 00027
, 0.00025
/JO, 531
2.05
16

-------
                                 Table 7 '
                                                  i
                FACILITY A3 (Secondary Outlet-Fluorides)

                           Summary of Results
 Run number

 Date

 Test Time-minutes
  ~ -• 7' r-      -- ' •    '     '.'•-.••
 Production rate - TPH  .

 Stack Effluent

   Flow rate - DSCFM

   Flow rate - DSCF/tpn

   Temperature - °F

   Water vapor - Vol. %

   C02 - Vol. % dry

   02  - Vol. % dry

   (&*.'- Vol. % dry

 Visrit»ie Emissions - % opacity

 Fluorides

   Soluble
   ~' "   r  """"""  t

     gr/DSCF               ' ;?

  ^' ;gr/AGF

     Ib/hr

   de Ib/ton ofvtprbduct    •;'

 Total Fluorides

 • -   Sr/DSCF     -

•'•-•'-   gr/ACF

.  -: lb/hr

     Ib/ton of product


 Reference 3.
  3/10/72
  2           3       Average

3/14/72    3/16/72       -_  '
0.000193     0.000169    0.000170    0.000177
     V.49
   1.31
1.31
1.37
                                                                           17

-------
                                   Table 8
                   FACILITY A4  (Secondary Outlet-Fluorides)
                             Summary of Results .
    Run number
    Date
    Test Time-minutes
    Production rate - TPH
    Stack Effluent
      Flow rate - DSCFM
      Flow rate - DSCF/ton
      Temperature - °F
      Water vapor - Vol.  %
      C02 - Vol.  % dry
      02  - Vol.  7. dry
      CO  - Vol.  % dry
    Visible Emissions - % opacity
    Fluorides
      Soluble
        gr/DSCF
        gr/ACF
        Ib/hr
        Ib/ton of product
                  .  r t '^
   Total  Fluorides
        gr/DSCF
        gr/ACF
        Ib/hr
        Ib/ton of product
   *  Average of 32  tests.
   Reference'5.
   Average*
io'
     1.5.2
18

-------
 Run:-nuftiber-:              .  •




•Date -•  -




 Test Time-minutes




 Production rate - TPH




 Stack Effluent




   Flow"rate - DSCFM




   Flow-rate - DSCF/ton




   Temperature - °F




   Water  vapor - Vol. %




   C02 -  Vol. 7o dry




   02  -  Vol. 7.'dry




  . CO  •* Vol. 7. ,dry




 Visible' Emissions - % opacity




 Fluorides




   Soluble        .   -    ,




     gr'/DSCF




     gr'/ACF     •




     Ib'/hr




    , lb/ton of product




 Total Fluorides       • .




     gr/DSCF




     gr/ACF




     IbVhr      .




     Ib'/t'on of product






 Reference "5.
-Table 9
' (Primary



Outlet, - 'Fluorides)
ta'ry- o'f Results | .
1
5/15/72
240
0.441

50,596
115,000
57.4
5.42
0.6
20.2
D.O
107.

0.00040

0.00039
0. 174
0.394'
0.00042
0.00040
0.181
0. 410
:2
5/12/72 ;
240 [
0.441
i-
48,795
111,000 '
I.
57,6
5.76
0.6
20.2 '!
0.0 '
i
,
0.00039

0.00031:
0.162 ,
6.365
' I
0.00044
0.00033
0.169
0.382 ;
V
i
K
• i
3
5/16/72
240
0.441 -

47,121 ,
107,000
83.7
, .. 5.64
0.6
20. 2
.0.0
10%;

0.00046

0.00042
0.186
0;422
-• 0.00046
0.00042
0.186
0.422
Average
-
240
-0.441.
-fc«;* ,», ..;
48,837
111,000
66.3
5.61
0.6
20.2
0.0
107=
-' -., -:' /-•
0.00043
,i: '.~ '
0.00038
6.174
6.394
6. '06 044
0.00038
0.179
0.405
                                                                              19

-------
                                   Table  10
                  FACILITY B,  (Primary  Outlet-Fluorides)
                           Jl
                             Summary  of  Results
   Run number
   Date
   Test Time-minutes
   Production rate - TPH
   Stack Effluent
     Flow rate - DSCFM
     Flow rate - DSCF/tpn
     Temperature .- °F
     Water vapor - Vol. %
     C02 - Vol. % dry
     02  - Vol. % dry
     CO  - Vol. % dry
   Visible Emissions - 7» opacity
   Fluorides
     Soluble
   Range
Average
                                                    f ir: .•}•":
       gr/DSCF
       gr/ACF
       Ib/hr
       Ib/ton of product
   Total Fluorides
  V   1gr/DSCF
       gr/ACF
       Ib/hr
       Ib/ton of product
  Reference 7.
0.43 to 0.62
  Cf.50'
20

-------
                                      Table  11;
                        FACILITY - B (Roof-Emissions-Fluorides]
                                  Summary of Results           !
Run Number

Date

Test Time-minutes

Production rate - TPH
 I     '        ' .    -       '  •
Stack Effluent
 i
 i Flow rate - DSCFM

 j Flow rate - DSCF/ton

 | Temperature °F

 , Water vapor - Vol. %

  C02 - Vol. % dry

  02  - Vol. %. dry

 ' CO  r Vol. % dry

Visible Emissions - % opacity

Fluorides

 ! Soluble
 i  •
 !   gr/DSCF    '     .
 !     ,  "
    gr/ACF
 •I..'--
 ;   lb/hr
 l             '   - •
 1   Ib/ton of product

  Total Fluorides

 ;   gr/DSCF  'x

 j  •, gr/ACF         ,
 i   .  •  .    '    '..'•.        -
 j   lb/hr' '               ,  ' '

 j   Ib/ton of • product    ,'
 i     . :      •-•.'.••..
 i             •       •',-:'•
 /Reference 6.
.; i . ' :
5/12/72 ,
1062
2.64
2,811,000
1,065,000
75 •:•••
0
0.7
19.9
0.0
0
0.00012
0.00012
2.87
1.09
0.00012
0.00012
2.92
1.10
2
5/15/72
735
2.64
2,811,000
1,065,000
70
0.87
0.7
19.9
0.0
0
0.00021
0.00021
5.12 .
1.93
0.00022
0.00022
5.32
2.01 ,
3
4
Average
5/16/72 5/17/72 ''" ' -
645
2.64
2,811,
1,065,
70
0.95
0.7
19.9
0.0
0
450
2.64
000 2,811,000 T
000 1,065, 000 :
65
0.64
0.7
- '. ,.'-;,
1.9.9
0.0
0
0.00024 0.00030
- 0.00024 0.00030
5.87
2.22
7.30
-
f..2.76
0.00025 0.00031 .•,...;
0.00025 0.00031
6.04
2.28
7.54
2.85 ;
723
"2.64'
2,811,00
1,065,00
89
0.62
0.7
19.9
0.6
0
, 0.00022
0,00022
5.29
2.00
0.00022
0. 00022
5.45
2.06
                                                                                    21

-------
                                   Table  12
                     FACILITY B]  (Roof Emissions-Fluorides)
                              Summary of  Results
    Run number
    Date
    Test Time-minutes
    Production rate - TPH
    Stack Effluent
      Flow rate - DSCFM
      Flow rate - DSCF/ton
      Temperature - °F
      Water vapor - Vol. 7,
      C02 - Vol. 7. dry
      02  - Vol. % dry
      CO  - Vol. % dry
    Visible Emissions - % opacity
    Fluorides
      Soluble
        gr/DSCF
        gr/ACF
        Ib/hr
        Ib/ton of product
    Total Fluorides
        gr/DSCF
        gr/ACF
        Ib/hr
        Ib/ton of product
     Reference 7.
    Range
Average
0.91 to 1.68
 1.15
22

-------
                                     Table 13               j




                     FACILITY -  C   (Primary Outlet - Fluorides)




                               Summary of Results
Run Number
Da'te ' '
Test Time-minutes
Production rate - TPH
Stack Effluent
'Flow rate - DSCFM
Flow rate '-. .DSCF/ton
Temperature °F
|Water vapor - Vol. %
C02 - Vol. % dry
t>2 - Vol. % dry
CO - Vol. % dry :
Visible Emissions - % opacity
Fluorides
^Soluble
gr/DSCF
i
gr/ACF ' . -
Ib/hr
Ib/ton of product
• total Fluorides
; gr/DSCF ' • ,.'
gr/ACF
Ib/hr'
Ib/ton of product
1*
5/1/72
336
0.122

10,334
5,170,000
192.2
0.00
0.0
19.8
0.6
0 .


0.000082 •

0.000065
0.00724
0.0592

. 0.000092
0.000073
0.00814
0.0667
. -- 2
5/2/72
384
0.123

10,51.2
5,260,000
179.1
.. - 0.00
0.0
19.8
0.6
0'


0.00.0365

0.0000290
0.0321
0.260

0.000374
0.000300
,0.0329
6.267
3 ; . 4*
5/3772 5/4/72
384 ' 384
0.124! 0.124

10,532
5,280,0(
176.1
0.33
0.0
19.8
,0.6
o

9,389
0 4,690,000
181.0
0.49
0.0
19.8
0.6
0
i- -

0.00023 0.000084

0.00019 0.000068
0.0210 0.0068
,0.168 0.055

0.00023C 0.000084-
0.000190 0.000069
0.0210 0.00068
0.168 0.055
Average
-
123.3
123.3

10,192
5,100,000
182.1
0.21
0.0
'. 19.8
0.6
0


.0.000190

0.000153
0.0168
0.'135

.= 0.000195
0. 000158
0.0172
0.139
*  Deleted from use in standard data.
Reference 8.
                                                                                  23

-------
               Table 14




FACILITY - C (Roof Emissions - Fluorides)



          Summary of Results
Run Number
'Date
Test Time-minutes
Production rate - TPH
Stack Effluent
Flow rate - DSCFM
Flow rate - DSCF/ton
Temperature °F
Water vapor - Vol. %
C02 - Vol. 7. dry
02 - Vol. 7. dry
CO - Vol. 7. dry
Visible Emissions - % opacity
Fluorides
Soluble
gr/DSCF
gr/ACF
Ib/hr
Ib/ton of product
Total Fluorides
gr/DSCF
gr/ACF
Ib/hr
Ib/ton of product
Reference 8.
24
1
5/1/72
565
3.72

1,403,000
2,265,000
84.7
0.00
0.4
20.6
0.0
0


0.000173
0.000166
2.075
•1.12
•-'
0.000173
0.000166
2.075
1.12

aft...
2
5/2/72
1229
3.72

1,551,000
2,500,000
91.7
0.00
0.4
20.6
0.0
0


0.000188
0.000178
2.492
1.34

0.000191
0.000181
2.542
1.37

,• .' ',
3
5/3/72
1377
3.72

1,407,000
2,275,000
' 106.3
0.291
0.4
20.6
0.0
°'!


0.00186
0.000171
2.244 ,
1.21

0.000188
0.000174 :
2.284
1.23 .
,'
, ;' .
, 4
5/4-5/72
1350
3.72

1,492,000
2,410,000
' 106.5
0.110
. 0.4
20.6
0.0
0

'.''• ' '•'
0. 000158
0.000146
2. 022
1.09

0.000160
0.000148
2.050
1.10


Average
-
1130
3.70

• 2,362,500
1,463,250
97.3
0.10 '
0.4 '
20.6
0.0
0


0.000176
0.000165
2.208
1.19

0.000178
0.000167
2.238
1.20



-------
Table 15
(Primary

Outlet -
nmary of Results
1 . •' '
2/29/72
192
0.449
19,579 .''.
43,650
239
0.514
3.40
16.3
0.3
0
0.0015
0.0011
0.252
0.561
0.0016 .. ... •
0.0012
0.276
0.612
2*
3/1/72
192
0.449
18,162
44,850
228
1.358
3.40
16.3
0.3
0
0.0042
0.0031
0.720
1.560
0.0043
0.0032
0.744
1.656

Fluorides)
. , ' . i •-
3*. Average
3/1/72
., 192 , 192
0.449 n .-.-0.44.9 „..,
19,711 19,150
43,950 44,150
.237 234
1.36 1.Q8
3.4 3.4
16.3. 16.3 '
0.3 , 0.3
0 0
0.0042 .0.0033 '
0.0031 0.0024
0.234 • 0.402
1.560 1.23
0.0043 , 0.0034
0.0031 . 0.0025
0.240 ' 0.42
1/602 1.29
    , v,Run  number


     Date


     Test Time-minutes


     Production rate - TPH


    .Stack Effluent


    ,  . Flow rate - DSCFM         '.


      , Flow'rate - DSCF/ton


       Temperature - °F


       Water vapor - Vol.  %


       C02-- Vol.  % dry    '     ,  '


       02   - Vol.  % dry

       CO   -;Vol.  % dry    :


    Visible  Emissions  - %' opacity

    Fluorides


     . Soluble


      •  gr/DSCF


       ' gr/ACF               .   /


        Ib/hr


        Ib/ton of product

    Total Fluorides


        gr/DSCF


        gr/AGF


        Ib/hr    '


        Ib/ton of product
*  Operator experienced feed control  problems  this  date.   Malfunction  corrected
   before next test.   This data questionable and  deleted  from  use  in standard
                                                                              25

-------
                                  Table 15  (Continued)




                   FACILITY -   D  (Primary Outlet -  Fluorides)



                             Summary of Results
 Run number



 Date



 Test Time-minutes



 Production rate - TPH



 Stack Effluent



   Flow rate - DSCFM



   Flow rate - DSCF/ton



   Temperature - °F




   Water vapor - Vol. %



   C02 - Vol. % dry



   02  - Vol. % dry



   CO  - Vol. % dry



 Visible1Emissions - % opacity



 Fluorides



   Soluble



     gr/DSCF



     gr/ACF



     Ib/hr




     Ib/ton of product



 Total Fluorides



     gr/DSCF



     gr/ACF



     Ib/hr



     Ib/ton of product




Reference 9.




26
4
3/2/72
192
0.449
V
19,313
43,050
233
1.54
3.4
16.3
0.3

0
0.0013
0.0010
0.072
0.483
0.0014
0.0010
0.078
0.519
5
3/2/72
192
0.449

20,976
46,650
235
0.97
3.4
16,3
0.3

0
0.0012
0. 0009
0.072
0.477
0.0013
0.0009
0.075
0.504
6
3/3/72
192
0.449

19,598
43,800
225
1.31
3.4
16.3
0.3
;•--.'•
,0
0.0008
0.0006
0.135
0.297
0.007
0.0007
0. 147
0.321
Average
.'-
192
0.449

19,962
44,500
231
1.28
3.4
16.3
0.3

0 .
0.0011(
0.0008
0.093
,mi
0.0011
0, 0008
0.100
0.448

-------
      Run number


      Date       •     '          -.


 •     Test Time-minutes


      Production rate  -  TPH


      Stack Effluent


       Flow rate - DSCFM


     ,, Flow.rate - DSCF/ton


       Temperature -  °F


       Water vapor -Vol.  %


       C02 - Vol. % dry


       02  - Vol. % dry


       CO  - Vol. % ,dry'"

                        "t.   •
     Visible Emissions  - %  opacity


     Fluorides       '      .   '


       Soluble


         gr/DSCF      '.'

         gr/ACF      ;   --•---••••


         ib/hr        ''.''.


         Ib/ton of  product


     Total Fluorides               '


       '  gr/DSCF


       'gr/ACF              '  .


         Ib/hr    ;        '


         Ib/ton of product


Reference 9,
Table 16
D]_ (Primary
-
Outlet -

Fluorides)
rnnary of Results '
1
3/6/72
192
0.449
2.
3/7/72
192
0.449
19,671.3 18,868.2
43,800 42,000 •
209.8
0.374
3.4
16.3
0.3
o

0.0012
0. 0009
0.1998
0.484
0.0013
0.0010
0.2223
0.495
216.3 ,
0. 353
3.4
16.3 !
K
0.3
o !,.
• "f
0,0009
0.0007
0,1506
0.336
0.0011
0. 0008
0.1710
0.381
3 , Average
3/7/72 -
192 192
0.449 0.449
18,903.00 19,147.00
42,150 42,650
221.3 215.8
0.700 0.476
3.4 3.4
16.3 16.3 ,
0.3 0.3
0 0

0.0011 0.0011
0.0008 0.0008
0.1761 0.1755
0.393 0.404
0.0012 0.0012
0.0009 0.0009
0.1968 0.1967
0.438 0.438
                                                                             27

-------
 Date:
 Type of Plant:
 Type of Discharge:
 Location of Discharge:
 Height  of  Point of Discharge;
 Description of Background:
                                    table  17
                                   FACILITY  D
                          SUMMARY OF VISIBLE EMISSIONS

                     2/20/74
                     Primary Aluminum Plant (Potroom Facility)
                     stacks (14)           Distance from Observer to Discharge Point:
                     Top  of baghouse

                       50  ft.

                     sky
                                                                      150 ft.

                          Height  of Observation Point:                groun'd level

                          Direction of Observer from Discharge Point: SE
  Description  of Sky:
                               cleat
  Hind Direction:               SSW
  Color of Plume:               white
  Interference of Steam Plume:  none"
  Duration of Observation:      9  hours
                                          Wind  Velocity:
                                          Detached  Plume:
                                                             mi/hr'
  Summary of Data:
          Op'acity,
          Percent
              5
             10
             15
             20
             25
             30
             35
             40
             45
             50
             Total  Time Equal  to or Greater
                  Than Given Opacity	
                           !    Sec.
"HThT

  24
   2
   0
                                 45
                                 15
                                  0
                                Opaci ty,
                                Percent
 55
 60
 65
 70
 75
 80
 85
 90
 95
100
           Total  Time  Equal  to or Greater
               Than Given Opacity  .   • .<•
                                                                            M1n.
                                                                                          Sec.
  Sketch Showing How Opacity Varied With Time:
                                             .(D
   §   10
   £   5
   i   ,
                                              T
L
                                               4         5


                                               TIME, hours
  (1)  High points come from one stack out of the 14 and during periods-when  rapping was  occurring.
Reference 10.

28

-------
    Dates-
    Type of Plant:
    Type of Discharge:
    Location of Discharge:
    Height of Point of Discharge:  50  ft.

    Description of Background:     sky


    Description of Sky:          'clear


    Wind Direction:                NNE

    Color of Plume:                white
    Interference of Steam Plume:   none
    Duration of Observation:       8 hours
                         Table 18 ,                       ;:     •       ;

                        FACILITY  D'                     ;    '  .  ' -  ;

              SUMMARY OF VISIBLE EMISSIONS             i
                 "       -. '     .         •'          • :   :i    ,'.•"'••
          2/21/74     ,                                ;j

          Primary Aluminum ^plant  (Potroom Facilities) j

          stacks (14)         Distance from Observer tp  Discharge  Point:
          top of baghouse     Height of Observation  Point:
                              Direction of Observer from Discharge Point:  SE
                                                         150 ft.

                                                        ground level
                              Wind Velocity:
                              Detached Plume:
                              10-15'
                              no
                            mi/hr
Total Time Equal to or Greater
     Than Given Opacity
    M1n.

      9
      1
      0
Sec.

15
30
 0
    Summary of Data:
            Opacity,
            Percent
                5
               10
               15
               20
               25
               30
               35
               40
               45
               50
    Sketch  Showing  How Opacity VariedI  With  Time:
                 Opacity,
                 Percent
 55
 60
 65
 70
 75
 80
 85
 90
 95
100
           Total Time Equal to or Greater
           '•'. '  Than Given Opacity
                     ~	~
      •s  10

      ^  ?

      I  o
                                                            JD
                      .     •              -        • TIME, hours'   '.. '        •


    (1)  High points come_from one stack  out of the 14 stacks  and during  the  period when  rapping was occurring.

'                      .  •                              -           \ •''•••''          >•      ;.
'  Reference 10.                                                                                   •
                                                           '                          '

-------
                               Table 19




                  FACILITY-   D    (Roof Emissions-Fluorides)



                           Summary of  Results
Mun number
DiiCe
lest Time-minutes
Production rate - TPH
Stack Effluent
Flow rate - DSCFM
Flow rate - DSCF/ton
Temperature - °F
Water vapor - Vol. %
C02 - Vol. 7. dry
02 - Vol. 7. dry
CO - Vol. % dry
Visible Emissions - % opacity
Fluorides
Soluble
gr/DSCF
gr/ACF
Ib/hr
Ib/ton of product
Total Fluorides
gr/DSCF
gr/ACF
Ib/hr
Ib/ton of product
1
•3/1-2/72'
1441
1.740
(665,310)
382,000
105.9
0.0
1.8..
20.8
' 0.8
0 •
0.00022
0.00020
1.28
^0,73 ~-.
0.. 00026
0.00024
1.50
0.86
2 3
3/2-3/72
1200
1.740
(754,152)
433,000
103.5
0.0
1.8
20.8
, 0.8
0
0.00036
0.00033
2.32
1>33_,,, _..,„,,._„,„.
0.00040
0.00036
2.57
1.48
Average
•••"-'. '.'
1320.5
" 1.740
709,731
407,500
104.7
0.0
1.8
20.8
0.8
-0
0.00029
0.00027
1.80
—t-M—
6. 00033
0.00030
2.04
1.17
 Reference 9.



30

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    Date:
    Type of Plant:
    Type of Discharge:
   ' Location of Discharge:
    Height  of Point of Discharge:  60  ft.
    Description of Background:     sky
                         Table 20 -.";.....''..

                :  -.   '  FACILITY .D  .      .   :'
              SUMMARY OF VISIBLE EMISSIONS

         2/21/74                             •
         Primary  Aluminum plant  (Potroom Facility)
         Monitor         "    Distance from Observer to" Discharge Point:   160ft.
         Roof of  potroom -     Height of Observation Point:                ground level
                              Directipn of Observer from Discharge Point: southeast
    Description of Sky:
         clear
   Wind Direction:               NNE
   Color of Plume:               -
   Interference of Steam Plume:  none
   Duration of Observation:      8  hours
                              Wind Velocity:
                              Detached Plume:
                10-15
                no
                 mi/hr
   Summary of Data:
           Opacity,
           Percent
               5
              10
              15
              20
              25
              30
              35
              40
              45
              50
Total Time Equal to or Greater
     Than Given Opacity
	 Min.        ^5ic~	:

      Visible emissions' were
      consistently zero percent
      opacity.         '   '
Opacity,
Percent
   55
   60
   65
   70
   75
   80
   85
   90
   95
  TOO
Total'[Time Equal to or Greater
_^	Than Given Opacity 	
                                                                              Win.
                                Sec.
   Sketch Showing How Opacity Varied With Time:
i'  S   10
1   s.

'  I   5

  °   0
                            2         3         45


                             •  .    TIME, hours'  '
Reference 10.
                                                                                                           31

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                                              FACILITY  D

                                     SUMMARY OF VISIBLE EMISSIONS
  Date:
  Type of Plant:
  Type of Discharge:
  Location of Discharge:
         2/20/74
         Primary Aluminum plant  (Potroom Facility)

         Monitor              Distance from Observer to Discharge Point:

         roof of potroom      Height of Observation Point:
  Height of Point of Discharge: 60 ft.
  Description of Background:    sky
                                      160ft.

                                      ground,level
                              Direction  of Observer  from. Discharge Point: southeast
  Description of Sky:
                                clear
  Hind Direction:               NNW
  Color of Plume:
  Interference of Steam Plume:  none
  Duration of Observation:      ^
                              Wind Velocity:
                              Detached Plume:
               5-10, .
                no
  Surmary of Data:
          Opacity,
          Percent
              5
             10
             15
             20
             25
             30
             35
             40
             45
             50
Total Time Equal to or Greater
     Than Given Opacity '
                            M1n.
                   Sec.
Visible emissions were con-
sistently zero percent opacity.
Opacity,
Percent
   55
   60
   65
   70
   75
   80
   85
   90
   95
  100
Total Time Equal  to or Greater
   .  Than Given Opacity	:
                                                                             Min.
                                                                    Sec.
   Sketch Showing How Opacity Varied With Time:

1 is
i a
i i i i
— " _
— ' • . —
i i • i
1 2 3 4 56 7
                                     : TIME, hours'
Reference 10.

32

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                               Table 22

                 FACILITY E (Primary Outlet-Fluorides)

                          Summary of Results
-ei'V:1- ty.t-
 Run number

"Date' • \  •      ••-....

 Test Timerniinutes

 Production rate - TPH

 Stack' Effluent'-'"'

   Flow rate - DSCFM

   Flow rate - DSCF/tpn

   Temperature - °F

   Water vapor -'Vol. %

   C02 - Vol. % dry  ,

   02  .- Vol. % dry        ;:

   CO  - Vol. '% dry

 Visible Emissions - % opacity

 Fluorides
  i   f '   • :     ,
   Soluble .

     gr/DSCF            _.-„,

     gr/ACF
         Range of Data* ;
Average
    ,lb/tpn of product
         j__
 Total Fluorides

     gr/DSCF
     Ib/ton of product                 0.2 to. 1.0

 *  14 data points from tests at 2 plants.

 Reference 11.
                                         0.51
                                                                          33

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                               Table 23
                 FACILITY E (Roof Emissions-Fluorides)
                          Summary of Results
 Run number
 Date
 Test Time-minutes  •
 Production rate - TPH
 Stack Effluent
   Flow rate - DSCFM
   Flow rate - DSCF/tpn
   Temperature - °F
   Water vapor - Vol.  %
   C02 - Vol.  % dry
   02  - Vol.  % dry
   CO  - Vol.  % dry
 Visible Emissions - % opacity
 Fluorides
   Soluble
     gr/DSCF
     gr/ACF
     Ib/hr
     Ib/ton of product
 Total Fluorides
     gr/DSCF
     gr/ACF
     Ib/hr
     Ib/ton of product
   Range of Data*
Mid 1971 to Mid 1972
.Average
    0.83 to  1.31
  1.14
*  7 data points from tests at 2 plants.  A high value of 4.40 Ib/ton of product
   was deleted.                                                    •            '
Reference 11.

-------
                              Tab1e;24              :
                 FACILITY  F  (Primary Out!et-FTuoride
-------
                                  Table 25
                    FACILITY 6  (Primary Outlet-Fluorides)
                              Summary of Results*
    Run number
    Date
    Test Time-minutes
    Production rate - TPH
    Stack Effluent
      Flow rate - DSCFM
      Flow rate - DSCF/ton
      Temperature - °F
      Water vapor - Vol. %
      C02 - Vol. % dry
      02  - Vol. % dry
      CO  - Vol. % dry
    Visible Emissions - % opacity
    Fluorides
      Soluble
        gr/DSCF
        gr/ACF
        Ib/hr
        Ib/ton of product
    Total Fluorides
        gr/DSCF
        gr/ACF
        Ib/hr
        Ib/ton
Average
  7.3
  (L74
   *  Average of tests over 1 '1./2 years.
   References 12 and 13.
36

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                               Table 26         ;   •
                            •• •              "     i'    '

                FACILITY 6 (Roof Emissions-Fluorides)
                       -  •..'•'   .. •    •           !•   . •
                          Summary of Results     1
Run number


Date


Test Time-minutes


Production rate - TPH


Stack Effluent


  Flow rate - DSCFM


  Flow rate - DSCF/tpn


  Temperature - °F


  Water vapor - Vol. %


  C02 - Vol. % dry


  02  - Vol. % dry


  CO  - Vol. % dry


Visible Emissions - % opacity


Fluorides


  Soluble                   .


    gr/DSCF


    gr/ACF    '            ,


    Ib/hr


    Ib/ton of product


Total Fluorides


    gr/DSCF


    gr/ACF


    Ib/hr


   •Ib/ton of product


*  Average of tests  over 1  1/2  years.


References 12 and  13.
Average*
  11.7

   1.18
                                                                      37

-------
                                   Table 27  '
                     FACILITY H (Primary Outlet-Fluorides)
                              Summary of Results
     Run number
     Date
     Test- Time-minutes
     Production rate - TPH
     Stack Effluent
       Flow rate - DSCFM
       Flow rate - DSCF/tpn
       Temperature - °F
       Water vapor - Vol.  %
       C02 - Vol.  % dry
       02  - Vol.  % dry ,
       CO  - Vol.  % dry
     Visible Emissions - % opacity
     Fluorides
       Soluble
         gr/DSCF
         gr/ACF
         Ib/hr
         Ib/ton of product
     Total Fluorides
         gr/DSCF
         gr/ACF
         Ib/hr
         Ib/ton of product
     *  Average over a  6-month period.
     Reference 14.
Average*
  0.31
38

-------
                                Table  28


                 FACILITY H (Secondary Outlet-Fluorides)


                           Summary  of  Results



 Run number                                           l


. Date


 Test Time-minutes               .                   '


 Production rate - TPH


 Stack .Egfluent                  „              	.„,.


   Flow rate - DSCFM


   Flow rate - DSCF/tpn


   Temperature - °F                         .        i.


   Water vapor - Vol.  %


   C02 - Vol.  % dry


   02  - Vol.  % dry


   CO  - Vol.  % dry


 Visible Emissions - % opacity                      ]
                              •

 Fluorides


   Soluble                                          |  ' ,


     gr/DSCF            .       .                   •  :


     gr/ACF


     Ib/hr                                          i


^c   Ib/ton of.prpduct


 Total Fluorides


     gr/DSCF


     gr/ACF


     Ib/hr


     Ib/ton of product


 *  Average for ]8 months  of continuous,sampling.


Reference  14.
Average*
  1.18
                                                                          39

-------

-------
ANODE BAKE FURNACE
       DATA
         41

-------
                                  Table 29




                   FACILITY - A (Anode Furnace-Fluorides)




                             Summary  of Results
JRun number
Date
Test Time-minutes
Production rate - TPH (Anode)
-- . : .3 ', . '-
Stack Effluent
Flow rate - DSCFM
Flow rate - DSCF/ton
Temperature - °F
Water vapor - Vol. %
C02 - Vol. % dry
02 - Vol. % dry
CO - Vol. % dry
Visible Emissions - % opacity
Fluorides
Soluble
gr/DSCF
gr/ACF
Ib/hr
Ib/ton of anode
Total Fluorides

gr/DSCF
gr/ACF
Ib/hr
Ib/ton of anode
-1
6/20/72
224
9.1
),-»i'Z6iJ.\

38', 830
2,930
117.3
7.52
0.66
14.3
1.6
20


0.0182
0.0150
5.75
0.63
_-..-.
.5
0.0201
0.0166
6.35
0.70
2
6/21/72
140
9.1
fed Ms

44,620
3,550
125.2
7.36
0.66
14.3
1.6
20


0.0211
0.0173
8.06
0.89

j '
0.0221
0.0183
8.69
0.96
3
6/21/72
140
9.1
<

, 37,060
2,950
125.1
6.46
0.66
14.3
1.6
20


0.0206
0.0170
6.54
0.72


0.0216
0.0179
8.87
0.98
Average
- .
168
9;1
: v uifS to -<-
-------
   Date:
   Type of Plant:
   Type of Discharge:
   Location of Discharge:
Description of Sky:

Wind Direction:
Color of Plume:
Interference of Steam Plume:
Duration of Observation:
                                             Table 30                       |
                                            FACILITY  A                      ;
                                   SUMMARY OF VISIBLE EMISSIONS             !
                              2/25/74
                              Carbon Anode Bake Plant
                              stack                Distance from Observer to  Discharge  Point:
                              top of stack         Height of Observation  Point:
   Height of Point of Discharge:  181 ft.
   Description of Background:     sky
                                                                  250 ft.
                                                                 ground level
                     Direction  of Observer from  Discharge  Point:  North
                                 The sky was clear except for billowy white to gray clouds periodically
                                 crossing the sky.
W-WNW     .           Wind Velocity:      ,   8-10
white                Detached Plume:        no
yes, steam plume occurs at about 45°F.  The high was 27°
8 hours
                                                                                         nri/hr
   Summary of Data:
• Opacity, Total Time Equal to or Greater
Percent 'Than Given Opacity
Min. Sec.
5 480 0
10 0 0
'[ 15 r
• 20 - -
; 25
! 30 -
35 - -
1 40
.45 - -'
50
Opacity,
Percent

55
60
65
70
75
80
85
. 90
95
100
Total Time Equal
Than Given
Min.
.
'
i-
-
-
-
,-
i-
!-
-
to or Greater
Opacity
Sec.

_.
_
_
-
.
_
_
-
- .
   Sketch Showing How Opacity Varied With Time:
|i
i
                             2         3        4

                                     TIME, hours
  Reference 16.
                                                                                         -.:<.: 3 . •') I
                                                                                                          43

-------
                                             Table 31
                                             FACILITY A
                                    SUMMARY  OF  VISIBLE EMISSIONS
                               2/26/74
                               Carbon Anode Bake Plant
                               stack
Date:
Type of Plant:
Type of Discharge:
Location of Discharge:        top of stack
Height of Point of Discharge: 181 ft,
Description of Background:    sky
Distance from Observer to Discharge Point:    250  ft.
Height of Observation Point:                 ground level
Direction of Observer from Discharge Point:  east
 Description  of Sky:
                               clear
                                                                                        •J-J3U
 Wind Direction:                N-NNW
 Color of,Plume:              '  white  to  tan
 Interference of  Steam Plume:   yes
 Duration  of Observation:       6  hrs.

 Summary of Data:
                                                   Wind Velocity:
                                                   Detached Plume:
                   2-4

                   no
'mi/hr
Opacity,
Percent

5
10
15
20
25
30
35
40
45
50
Total Time Equal
Than Given
Mln.
360
351
353
2
0
-
-
-
-
-
to or Greater
Opacity '
Sec.
0
0
0
0
-
-
-
-
-
-
Opacity,
Percent

55
60
65
70
75
80
85
90
95
100
Total Time Equal
Than Given
Min.
.
_
• _
,
• , '
-
-
-
-
-
to or Greater
Opacity
Sec.

„
_
_
-
_
-
-
-
-
 Sketch Showing How Opacity Varied  With  Time:

20
IS
5
0

1 1 1
~ I —
|
_ll 1 ,
* Q p ? ? 0 1 *"*
I I I I !
Reference 16.
                                    34

                                    TIME, hours
                                                                                              .,J\dI

-------
                                  Table/'32'



                   FACILITY - B (Anode Furnace-F'mori ties)





                            Summary  of Results
Run number    • •    '      ' '"  •''-




Date




Test Time-minutes




Production rate - TP11  (Anode)




Stack Effluent




  Flow rate - DSCFM




  Flow rate - DSCF/ton




  Temperature - °F




  Water vapor - Vol. %




  C02 - Vol. 7. dry




  02  - Vol. 7. dry




  CO  - Vol. 7, dry




Visible Emissions - % opacity




Fluorides




  Soluble                . .
    gr/DSCF




    gr/ACF




    Ib/hr




    Ib/ton




Total Fluorides




    gr/DSCF




    gr/ACF ^




    Ib/hr




    Ib/ton of anode
••-'I. ----- „
10/19/72
240
13.15
75,774
5,162 ......
196
3.5
1.1
19.1
0.0
10-207.
-
0.02555
0".02002.
16'. 58
1.26
2
10/19/72
240
.13.15
72,460
5,510.
215
3-7
1.1
19.1
0.0
10-207.
-
0.02708
0.02056 •
16.81.
1.28
' 3 Average.
10/20/72
240 240
13.15 13.15
70,340 72,858
5,349 5,540
206
3.2 3.5
1.1 * 1.1
19.1 * , 19.1
0.0 * 0.0
10-207. 10-207.
t" : - . -
0.02605 0.02627
0.02027 0.02019
15.69 16.36
1.20 1.25
 *• ORSAT analyzer wa's not operating  properly.   This data questionable.



 Reference 17.'

-------
                                  REFERENCES
  Aluminum  Reduction  Facilities

  1.  Joint Emission  Test Report, October 24, 1972, EPA and Valentine, Fisher,
     and Tomlinson,  Contract No. 68-02-0236, EMB Test No. 72-MM-07.
  2.  Joint Emission  Test Report, EPA and Valentine, Fisher, and Tomlinson,
     Contract No. 68-02-0236, -EMB Test No. 73-ALR-l.

  3.  Memo  and attachments from David J. Lutrick, EPA Region X, to Reid E.
     Iversen, EPA, Applied Technology Division, June 9, 1972.

  4.  "Emissions from the Wet Scrubber System at [Plant A]," June 7, 1972,
     prepared for EPA by York Research Corporation, EMB Test No. 71-MM-21.
  5.  Data submitted  to EPA by the owner of Plant A.

  6.  Joint Emission Test Report, EPA and Valentine, Fisher, and Tomlinson,
     Contract No. 68-02-0236, EMB Test No.  72-MM-08.

  7.  Letter from a Division Engineer of the company operating Plant B to Reid
     Iversen, EPA, October 18, 1972.
  8.  Joint Emission Test Report, October 24, 1972,  EPA and Valentine, Fisher,
     and Tomlinson, Contract No. 68-02-0236, EMB Test No.  72-MM-06.

 9.  EPA Emission Testing Report No. 72-MM-12.
10.  Iversen, Reid E. ,  EPA, "Trip Report to [Plant  D]"  and attachments,  March 55
     1974.

-------
                                       -  2 -
 .11.   Letter from a Vice President of  the  company operating Plants C and D to
      Reid Iversen, EPA, September 15,  1972.

 12.   Pfaff,  Roger 0.,  EPA,  International  Trip Report and attachments,
      September 21, 1972.

 13.   Data  supplied to  EPA by the  owner of Plant 6.     \     •
                      .
 14.   Letter from  the State of Oregon Department of Envf ronmental Quality,
      August 7, 1973.
Anode Bake Furnaces                                    j
                                                       ^
                                                       j
15.  EPA Emission Test Report No. 72-MM-24.

16.  Iversen, Reid E., EPA, "Trip Report to  [Anode Facility B]"  and  attachments,
     March 5, 1974.
                                                       l
17.  Emission Test Report,  January 29,  1973,  prepared  for  EPA  by Midwest Research
     Institute, Contract No.  68-02-0228,  EMB  Test  No.  73-ALR-3.

-------
                                    TECHNICAL REPORT DATA
                            (Please read Instructions on the reverse before completing)
 REPOHT NO.
 EPA-450/2-74-020b
                                                            3. RECIPIENT'S ACCESSION-NO.
 TITLE AND SUBTITLE
  Background Information for Standards of Performance:
  Primary  Aluminum  Plants, Volume  2, Summary of Test
  Data
               EPORT DATE
               October  1974
             6. PERFORMING ORGANIZATION CODE
 AUTHOR(S)
                                                             8. PERFORMING ORGANIZATION REPORT
 . PERFORMING ORGANIZATION NAME AND ADDRESS
  U.S.  Environmental  Protection  Agency
  Office of Air Quality Planning and Standards
  Research Triangle Park, N.C.   27711
                                                             10. PROGRAM ELEMENT NO.
             11. CONTRACT/GRANT NO.
 2. SPONSORING AGENCY NAME AND ADDRESS
                                                             13. TYPE OF REPORT AND PERIOD COVERED
                                                             14. SPONSORING AGENCY CODE
 5. SUPPLEMENTARY NOTES
 8. ABSTRACT
  This volume  is  the first  of a series on  standards of  performance for  primary
  aluminum plants.   This volume presents the proposed standards and the rationale
  for the degree  of control  selected.  The volume also  discusses the  analytical
  methods for  sampling emissions and the environmental  and economic impact of
  the standards.
                                 KEY WORDS AND DOCUMENT ANALYSIS
                   DESCRIPTORS
                                                b.lDENTIFlERS/OPEN ENDED TERMS
                                                                           c.  COSATI Field/Group
   Air pollution
   Pollution control
   Performance standards
   Primary Aluminum Plants
      Air pollution  contnl
 18. DISTRIBUTION STATEMENT

   Unlimited
19. SECURITY CLASS (ThisReport/
  Unclassified	
                                                                            21. NO. OF PAGES
                                                20. SECURITY CLASS (Thispage)
                                                  Unclassified
                                                                            22. PRICE
EPA Form 2220-1 (9-73)


48
U.S. GOVERNMENT PRINTING OFFICE! 1974 - 640-877^622 - Region 4

-------

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