EPA-450/3-77-050 a
December 1977
    ENERGY REQUIREMENTS
           FOR CONTROLLING
                SO2 EMISSIONS
           FROM COAL-FIRED
            STEAM/ELECTRIC
                 GENERATORS
   U.S. ENVIRONMENTAL PROTECTION AGENCY
      Office of Air and Waste Management
    Office of Air Quality Planning and Standards
   Research Triangle Park, North Carolina 27711

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                                     EPA-450/3-77-050
       ENERGY REQUIREMENTS
FOR CONTROLLING SO2 EMISSIONS
            FROM COAL-FIRED
  STEAM/ELECTRIC GENERATORS
                        by

                      W.C. Thomas

                    Radian Corporation
                      P.O. Box 9948
                    Austin, Texas 78766
                   Contract No. 68-02-2608
                      Project No. 8
                EPA Project Officer: K.R. Durkee
                      Prepared for

             ENVIRONMENTAL PROTECTION AGENCY
               Office of Air and Waste Management
             Office of Air Quality Planning and Standards
             -Research Triangle Park, North Carolina 27711

                     December 1977

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This report is issued by the Environmental Protection Agency to report
technical data of interest to a limited number of readers.  Copies are
available free of charge to Federal employees, current contractors and
grantees, and nonprofit organizations - in limited quantities - from the
Library Services Office (MD-35), Research Triangle Park, North Carolina
27711;  or,  for a fee. from the National Technical Information Service,
5285 Port Royal Road, Springfield, Virginia 22161.
This report was furnished to the Environmental Protection Agency by
Radian Corporation, P.O. Box 9948, Austin, Texas 78766, in fulfillment
of Contract No. 68-02-2608,  Project No. 8.  The contents of this report
are reproduced herein as received from Radian Corporation.  The opinions,
findings, and conclusions expressed are those of the author and not
necessarily those of the Environmental Protection Agency.  Mention of
company or product names is not to be considered as an endorsement
by the Environmental Protection Agency.
                   Publication No. EPA-45G/3-77-050
                                 11

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                       TABLE OF CONTENTS
                                                          Page
Figures	    v
Tables	   vi
Abbreviations	  vii
Metric Conversion Factors	   ix

1.0       INTRODUCTION	    1
          1.1  Background	    1
          1. 2  Approach	    2
          1.3  Summary of Results	    2

2.0       CONCLUSIONS	,  	    8

3.0       DESIGN ASSUMPTIONS	   10
          3.1  Power Plant Design and Operating
               Assumptions	   10
          3.2  Emission Control System Design
               Assumptions	   11
               3.2.1  Design Assumptions for
                      FGD process	   14
               3.2.2  Design Assumptions for Physical
                      Coal Cleaning	   19
               3.2.3  Design Assumptions for
                      Coal Transportation	   20

4.0       RESULTS	   22
          4.1  SOa Control Systems Comparison	   22
               4.1.1  Comparison by SOz Control Level...   30
               4.1.2  Comparison by Coal Used/	   36
          4. 2  Energy Penalty Proj ections	   39

REFERENCES	   45
                              111

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                     CONTENTS (Cont'd)
APPENDIX A
APPENDIX B
APPENDIX C
APPENDIX D
APPENDIX E
APPENDIX F
APPENDIX G
LIMESTONE FGD PROCESS	
LIME FGD PROCESS	
MAGNESIA SLURRY FGD PROCESS	
WELLMAN-LORD/ALLIED FGD PROCESS
DOUBLE-ALKALI FGD PROCESS	,
PHYSICAL COAL CLEANING	
COAL TRANSPORTATION	
Page
 A-l
 B-l
 C-l
 D-l
 E-l
 F-l
 G-l
                              IV

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                            FIGURES

                                                            Page
Figure 1-1.  Energy penalties for S02 control - summary
             of effects of S02 control level	    6

Figure 4-1.  Energy requirements for SO2 and particulate
             control - 0.52 g S02/MJ control level,
             500 MW plant		   32

Figure 4-2.  Energy penalties for. S02 and particulate
             control - 0.52 g S02/MJ control level,
             500 MW plant	   34

Figure 4-3.  Energy requirements for S02 and particulate
             control - 0.22 g S02/MJ control level,
             500 MW plant	   35

Figure 4-4.  Energy requirements for S02 and particulate
             control - 3.570 sulfur coal, 500 MW plant	   37

Figure 4-5.  Energy requirements for S02 and particulate
             control - 7.0% sulfur coal, 500 MW plant	   38

Figure 4-6.  Energy requirements for S02 and particulate
             control - low heating value Western coal,
             500 MW plant	   40
Figure 4-7.  Energy requirements for S02 and particulate
             control - high heating value Western coal,
             500 MW plant	   41
                                v

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                            TABLES
                                                            Page
TABLE 1-1.   MODEL S02 EMISSION CONTROL SYSTEMS STUDIED....   3
TABLE 1-2.   ENERGY PENALTIES ASSOCIATED WITH DIFFERENT
             METHODS OF CONTROLLING S02 EMISSIONS		   4
TABLE 3-1.   COMPOSITIONS AND HEATING VALUES OF THE MODEL
             SYSTEM BOILER FUELS	  12
TABLE 3-2.   COMBUSTION CALCULATION ASSUMPTIONS AND
             RESULTS	  13
TABLE 3-3.   PROCESS DESIGN BASES FOR FGD PROCESSES	  16
TABLE 3-4.   COMPOSITIONS OF PHYSICALLY CLEANED COALS	  20
TABLE 4-1.   MODEL S02 EMISSION CONTROL SYSTEMS STUDIED....  23
TABLE 4-2.   ENERGY REQUIREMENTS FOR THE PROCESSING
             OPERATIONS IN FGD SYSTEMS	  25
TABLE 4-3.   COMPARISON OF TOTAL SYSTEM vs. "BARE BONES"
             SYSTEM ENERGY REQUIREMENTS	  26
TABLE 4-4.   ENERGY PENALTIES FOR MODEL S02 CONTROL SYSTEMS
             USING LIMESTONE SCRUBBING	  27
TABLE 4-5.   ENERGY PENALTIES FOR MODEL S02 CONTROL SYSTEM
             USING LIME SCRUBBING	  28
TABLE 4-6.   ENERGY PENALTIES FOR MODEL S02 CONTROL SYSTEMS
             USING MAGNESIA SLURRY, WELLMAN-LORD/ALLIED
             AND DOUBLE-ALKALI SCRUBBING	  29
TABLE 4-7.   PROJECTED S02 EMISSION CONTROL ENERGY
             PENALTIES--19 8 7	  42
TABLE 4-8.   PROJECTED S02 EMISSION CONTROL ENERGY
             PENALTIES--199 7	  43
                              vi

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                     LIST OF ABBREVIATIONS
acf
Btu
cf
D-A
EPA
exp
°F
FD
FGD
g
gal
GJ
HP
hr
ID
J
°K
kg
kJ
km
kW
L
LS
m3
MAF
MgO
MJ
MW
Nm3
NSPS
OAQPS
actual cubic foot
British thermal unit
cubic foot
double-alkali FGD
Environmental Protection Agency
exponent
degree Fahrenheit
forced draft
flue gas desulfurization
gram
gallon
gigajoule
horsepower
hour
induced draft
joule
degree Kelvin
kilogram
kilojoule
kilometer
kilowatt
lime FGD
limestone FGD
cubic meter
moisture ash free
magnesium oxide FGD
megaj oule
megawatt
normal cubic meter
New Source Performance Standard
Office of Air Quality Planning and Standards
                              VI1

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ROM
rem
s
scf
scfh
stm
TVA
W-L/A
yr
       ABBREVIATIONS  (Cont'd)

run-of-mine
removed
second
standard cubic foot
standard cubic foot per hour
steam
Tennessee Valley Authority
Wellman-Lord/Allied FGD
year
                             vnx

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                   METRIC  CONVERSION  FACTORS
      To Convert From
British thermal unit  (Btu)
degree Fahrenheit  (°F)
cubic foot  (ft3)
gallon (gal)
horsepower  (HP)
hour (hr)
inch (in) of H20
mile (mi)
pound (Ib)
        To
joule  (J)
degree Kelvin  (°K)
cubic meter (m3)
cubic meter (m3)
watt (W)
second (s)
pascal (Pa)
meter  (m)
gram (g)
 Multiply by
1055
K=(F+460)/1.8
0.02832
0.003785
746.0
3600
249.1
1609
453.6
            Multiplication Factors
                      103
                      106
                      109
                 Symbol
                    k
                    M
                    G
                                ix

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1.0
INTRODUCTION
          This report summarizes work done by Radian Corporation
for EPA under Contract 68-02-2608, task 8.  It describes the
energy penalties associated with the control of S02 emissions
from coal-fired power plants.
1.1
Background
          The existing New Source Performance Standard (NSPS)
for S02 emissions from coal-fired steam generators is 0.52 g
S02/MJ (1.2 Ib S02/106 Btu) of heat input.  Depending on coal
sulfur content and heating value, compliance with this standard
can be achieved by means of flue gas desulfurization (FGD),  coal
desulfurization, the use of low sulfur coal, or a combination of
these approaches.  Since the promulgation of the S02 NSPS in
1971, advances have been made in the performance and reliability
of FGD processes.  Because of .these advances, public interest
groups have requested t.hat the EPA promulgate more stringent
S02 emission standards.  Therefore, the EPA's Office of Air
Quality Planning and Standards (OAQPS) has undertaken a program
to review the existing NSPS.  The results of this program will
be used to determine whether the NSPS should be revised.
          This report is provided by Radian Corporation to assist
OAQPS in the review of the NSPS.  It addresses the energy penal-
ties which result from employing various control methods to re-
duce S02 emissions to certain specified levels.  In addition,
it compares energy requirements for S02 control to projected
total U.S. energy consumption in 1987 and 1997.

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1.2
Approach
          The study approach was based on an EPA model including
102 systems which are combinations of power plants and S02 con-
trol methods.  The variables considered in the model-are level
of S02 control, method of S02 control, power plant size, and
coal composition.  The levels of each variable considered in
this study and the combinations of variables were defined by
EPA as shown in Table 1-1.  Three levels of S02 control were
considered.  They include the existing NSPS (0.52 g S02/MJ heat
input), 90 percent S02 removal, and 0.22 g S02/MJ.  Control
methods considered include regenerable FGD processes,  nonregen-
erable FGD processes, transportation of low sulfur coal to the
Midwest, and a combination of coal cleaning and nonregenerable
FGD processes.

          Base case energy requirements for each S02 control
method were calculated from material and energy balances.   The
base case was 90 percent S02 removal from the flue gas of a
500 MW power plant burning 3.5 percent sulfur coal.  Extrap-
olation factors which describe energy requirements in terms of
flue gas rate and S02 removal were defined.  The extrapolation
factors were used to calculate energy requirements for all the
power plant/SO2 control system combinations included in the
model.
1.3
Summary of Results
          The results show how energy penalties depend on con-
trol method, level of control, and coal composition.  It was
found that per kW of generating capacity, plant size had little
effect on energy penalties.
                              -2-

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           Table 1-2 shows the energy penalties  associated with
 different methods  of control of S02  emissions.   Energy  penalties
 are described in terms  of percent  of energy input  to  an. equiva-
 lent capacity uncontrolled power plant.  A range of energy penal-
 ties is  given.   The variations  are due  to  percent  sulfur in the
 coal,  level  of S02 control and,  to a small extent, plant size.
 For the  FGD  processes,  the high end  of  these ranges represents
 the most difficult control cases--combustion of 7  percent sulfur
 coal with 90 percent S02  removal.

           Table 1-2 shows that  the lowest  energy penalties  are
 associated with nonregenerable  FGD processes.

 TABLE 1-2.   ENERGY PENALTIES ASSOCIATED WITH DIFFERENT  METHODS
                   OF CONTROLLING S02  EMISSIONS
                                            Energy  Penalty
                                    (% Energy Input to Equivalent
                                      Uncontrolled  Power  Plant)
SO2 Control Method
Nonregenerable FGD processes
  (Lime, Limestone, Double-Alkali)

Regenerable Magnesia Slurry
 FGD process

Transportation of low Sulfur coal

Coal cleaning plus nonregenerable
 FGD process

Regenerable Wellman-Lord/Allied
 (W-L/A) FGD process
                                           3.0 -  4.5


                                           5.0 - 10.0

                                           5.5 -  6.5


                                          10.0 - 11.0


                                          12.0 - 25.0
                                -4-

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          Figure 1-1 shows how energy penalties depend on the
level of SO2 control.  Two levels of control are shown, the
existing standard and 90 percent S02 removal.  Ninety percent
removal is a more stringent level of control than the existing
standard.  Figure 1-1 shows that for most control methods the
energy penalty for achieving 90 percent removal is about 10-15
percent higher than  that required to meet the  existing NSPS.

          The results of the study also show that for combustion
of low sulfur western coal, 90 percent S02 removal requires up to
10 percent more energy than controlling emissions to 0.22 g S02/MJ
(0.5 lb S02/106 Btu) of heat input.   For low sulfur coals, 0.22 g
S02/MJ is more stringent than the existing NSPS but less stringent
than 90 percent removal.

          For a "bare bones" S02 control system, the energy re-
quired for flue gas reheat and particulate/chloride removal is
excluded from the limestone and lime systems.  This reduces the
energy requirements of these systems by 50 to 60 percent.  For
the double-alkali, magnesia slurry and Wellman-Lord/Allied pro-
cesses, the particulate/chloride removal operation is required
to prevent buildup of chlorides in the S02 scrubbing liquor.
However,  excluding flue gas reheat requirements would reduce the
energy required by the MgO system by 15 to 25 percent, the W-L/A
by about 10 percent and the double-alkali by about 50 percent.

          The energy penalties associated with S02 controls were
compared with projected total U.S. energy consumption for 1987
and 1997.  Depending on control level, method of control, and
sulfur content of coal, the energy required to control S02 emis-
                                           i
sions from new coal-fired power plants will be from 0.5 to 4.4
percent of total energy consumption in 1987.  In 1997 the energy
penalty ranges from 0.7 to 6.3 percent of projected consumption.
Assuming the majority of future S02  controls are limestone or lime
                               -5-

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   100-
    80-
         Physical Coal Cleaning and
         Limestone or Lime  FGD
                     ©
        Transporting Low Sulfur Western
        Coal to Midwest-No FGD
                     ©
                                               Basis:
500 MW plant;
2640 J/kW-s net heat rate;
3.5% sulfur,
27.9 MJ/kg coal
                              Double-Alkali FGD
                 0.52 g SOa/MJ
                      (NSPS)
                                        	.,	
                                        90% SO2
                                        Removal
                    Level of  Control of SOa Emissions
          Figure  1-1.   Energy penalties  for SOa  control -
              summary of effects  of SOa  control  level.
                                   -6-

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FGD systems, as is presently true, the ranges for 1987 and 1997
would be 0.5 to 0.7 percent arid 0.7 to 1.0 percent, respectively.

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2.0
CONCLUSIONS
          The objectives of this study were to identify and
compare the energy impacts of various levels and means of con-
trolling S02 emissions from coal-fired power plants.  These ob-
jectives were achieved by developing energy requirement data for
102 model power plant/S02 emission control systems selected by
the EPA.  The designs used in this study are believed to be
representative of those available to industry.  It should be
noted that in industry the design of a power plant/S02 emission
control system is based on economic considerations.  Site specific
economic considerations therefore will have an influence on the
data developed in this study.  However, it is believed that the
general conclusions resulting from this study are valid for the
majority of economic situations encountered in industry.

          Four major variables—plant capacity, coal sulfur con-
tent, level of S02 control and means of S02 control--were examined
to determine their effect on the energy required to control S02
emissions from coal-fired power plants.  The results of the
study indicate that per unit of generating capacity, power plant
size has little influence on the energy penalties associated with
S02 emission controls.  The effects of the other three variables
are discussed below.

          1)  For combustion of a 3.5 percent sulfur
              coal and use of an FGD process, the
              energy requirements for achieving 90
              percent S02 removal are 10-15 percent
              greater than for complying with the
              existing new source performance standard
              of 0.52 g S02/MJ (1.2 Ib S02/10S Btu) of
              heat input.   For coal sulfur contents
              greater than 3.5 percent,  the difference
                              -8-

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    in energy penalties for the two control
    levels decreases,  this is because as coal
    sulfur content increases, the percent S02
    removal required to comply with the existing
    NSPS also increases, reaching 90 percent
    removal for a coal sulfur content of about
    7 percent.

2)  From an energy viewpoint, the nonregenerable
    FGD processes — limestone, lime, and double-
    alkali--are the best means of controlling
    SOa emissions from coal-fired power plants.
    The range of energy requirements, as a per-
    cent of the energy input to .an equivalent
    uncontrolled power plant, for the S02 control
    methods examined are:
       Nonregenerable FGD processes   - 3.0 - 4.5%

       Regenerable FGD processes
          magnesia slurry             -   5 - 10%
          Wellman-Lord/Allied         -  12 - 25%

       Physical coal cleaning and use
        of limestone or lime FGD      -  10 '- 11%
       Transporting low sulfur
        western coal to the Midwest;
        no FGD
- 5.5 - 6.5%
    Variations are due mainly to percent sulfur
    in the coal,  level of SO2 control and to a
    lesser extent plant size.
                    -9-

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 3.0
DESIGN ASSUMPTIONS
           The  EPA selected 102  model power plant/S02  emission
 control  systems  for examination in this  study.   These model  sys-
 tems were  based  on combinations of the following variables:

           1)   Level of  Control  of S02 emissions
            .   •   0.52 g S02/MJ  (1.2 Ib S02/106 Btu) of
                  heat input (the existing  S02 NSPS)
                  90 percent S02 removal  by FGD
               •   0.22 g S02/MJ  (0.5 Ib S02/105 Btu) of
                  heat input

           2)   The means of controlling S02  emissions
                  Limestone slurry scrubbing
                  Lime slurry scrubbing
                  Magnesia  slurry scrubbing
                  Wellman-Lord/Allied sodium solution  scrubbing
                  Double-alkali  scrubbing
                  Physical  coal  cleaning
                  Use of low sulfur  western coal  in
                  a Midwest power plant

Other variables were power plant  capacity  and coal composition.
Four power plant  capacities  and five run-of-mine  coals were con-
sidered.  The  design assumptions  used in this study for the
model system power  plants  and S02 control methods are  discussed
in Sections 3.1 and 3.2, respectively.
3.1
Power Plant Design and Operating Assumptions
          Two high sulfur eastern coals and three low sulfur
western coals were used as boiler fuels.  In addition, for
several of the model control systems the two eastern coals
                              -10-

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were physically cleaned (40 percent sulfur removal) prior to
combustion.  The compositions and heating values of these seven
coals are listed in Table 3-1.  Combustion calculations were
performed for the first six coals listed in Table 3-1.  (See
Table 3-2.)  These flue gas compositions served as the bases
for estimating the energy requirements for the FGD processes.
A combustion calculation was not performed for the last coal in
Table 3-1 since the model power plant/S02 control systems which
used this coal did not require an FGD process for S02 control.

          The power plant capacities examined in this study are
assumed to be net capacities, -i.e.,, the capacity available after
providing for plant auxiliaries.  FGD processes also require
auxiliary energy in the form of steam and electricity.  If this
energy is obtained from the power plant, the net generating ca-
pacity of the plant will be lowered.  In the past, power plants
have generally been designed with fairly standardized net capa-
cities.  If these same standardized net capacities are desired,
allowances for the energy requirements of the FGD system must be
made in the design of the plants.  This should not pose any un-
usual design problems, but will increase the cost of the power
plant (CO-644).
3.2
Emission Control System Design Assumptions
          The design options for the SOa emission control tech-
niques selected for examination are representative of those that
are commercially available.  In actual practice, it might be
advantageous to make changes in design options as the emission
control parameters change.  However, for this study the same
design bases are used for all of the model SOa emission control
systems.  The design bases and assumptions used for the FGD and
                              -11-

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coal cleaning processes and for transporting western coal to
the Midwest are discussed in the following sections.
3.2.1
Design Assumptions for FGD Process
          There are six basic process operations in the lime-
stone, lime, MgO, Wellman-Lord/Allied and double-alkali FGD
processes:

             Raw material handling and feed preparation,
             Particulate/chloride removal,
             SO2 scrubbing,
             Reheat,
             Fans, and
             Sulfur disposal/recovery.

The raw material handling and feed preparation operation is de-
signed to receive, store and prepare makeup reagents for the
FGD processes.  This requires storage silos, conveyors, grinders,
mixers, slurry or solution preparation tanks and pumps.  The
lime and double-alkali processes use lime as the S02 sorbent or
precipitation reagent.  Facilities for calcining limestone to
produce the lime were not included in the design basis.  If these
facilities were included, the energy requirements of the raw
material handling and feed preparation operations would be in-
creased by about a factor of 50 (EN-587).  This in turn would
increase the energy requirements of the  lime and double-alkali
processes by about 25 percent.

          The energy required to extract, process and transport
the raw materials for the FGD processes were not included in
this study.   To examine this aspect of the FGD system energy
requirements would require defining the location of specific
                              -14-

-------
power plants and raw material producers, and is outside the
scope of this  study.

          The  design bases selected for the other processing
steps are summarized in Table 3-3.  The following sections
briefly discuss these selections.

          Particulate/Chloride Removal

          In the magnesium oxide, Wellman-Lord/Allied and double-
alkali FGD processes, particulates and chlorides must be removed
from the flue  gas prior to the S02 scrubbers.  This is required
because the S02 scrubbing liquors in these systems are regener-
ated and recycled.  If chlorides and particulates are removed
along with the S02, they will build up in the scrubbing liquor
and cause operational problems such as corrosion of equipment.
Although particulates can be removed by baghouse filters or elec-
trostatic precipitators, chloride removal requires a wet scrubbing
device.  For this study, venturi scrubbers were selected for
chloride removal.  The removal of particulates along with the
chlorides imposes no additional energy requirements.

          In the limestone and lime processes,  it is feasible
to remove particulates, chlorides and SOz simultaneously because
the particulates and chlorides will be purged from the scrubbing
liquor with the calcium sulfite/sulfate solids.  However, this
will result in increased levels of solids arid chlorides in the
recirculating  scrubbing liquor.   This in turn may cause opera-
tional problems and/or not be the optimum operating mode.  For
example,  chlorides in the scrubbing liquor reduce the alkalinity
available to sorb SQ2.  As the available alkalinity decreases,
the scrubbing  liquor recirculation rate must be increased, in-
creasing the power requirements for the SO2 removal operation.
A higher level of chlorides in the recirculating liquor may also
                              -15-

-------
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                 -16-

-------
cause corrosion problems.  Similarly, higher levels of solids
in the recirculating liquor may cause increased equipment erosion,
In light of these potential problems, venturi prescrubbers were
included in this study for the limestone and lime processes.

          SO2 Scrubbing

          There are many types of SOa absorbers available.  Often
the choice of absorber type is determined by the preference or
experience of the company designing the system.  The selection
of the S02 absorbers indicated in Table 3-3 was based upon two
criteria:

          1)  they have been used in commercial applications
              or demonstration tests and
          2)  data on the operation of the absorber were
              available in the open literature.

          Reheat

          Indirect steam reheaters were selected for all of the
FGD processes.  An alternative to this choice is combustion of
an auxiliary fuel, such as natural gas or fuel oil, and direct
injection of the hot combustion gases into the flue gas.   Steam
reheaters were chosen because of the availability of steam from
the power plant and the uncertainty of future natural gas and
fuel oil supplies.

          The minimum stack exit temperature:required to prevent
sulfuric acid mist formation and provide plume buoyancy is not
well defined.   Common practice,  and the design basis for this
study, is to reheat the scrubbed gas to achieve an exit temper-
ature of 353°K (175°F).  Changing the reheat temperature by a
few degrees can significantly effect this energy requirement.
                              -17-

-------
This in turn  can  effect  the  energy requirements of the whole
FGD process since reheat  accounts for  35  to 45 percent of the
energy requirements for nonregenerable FGD systems and 10 to 20
percent of the requirements  for regenerable FGD systems.
          Fans
          Either induced draft  (I.D.) or forced draft  (F.D.) fans
can be used to maintain gas flow through the scrubbing systems.
I.D. fans require about 10 percent less energy than F.D. fans.
However, a potential disadvantage of I.D. fans is their suscepti
bility to corrosion,if scrubbing liquor is entrained in the flue
gas exiting the S02 absorbers.  For this study, I.D. fans were
selected for all of the FGD processes because of their lower
energy consumption.

          Sulfur Disposal/Recovery

          The limestone, lime and double-alkali FGD processes
produce a calcium sulfite/sulfate sludge.  Ponding is the normal
on-site method of sludge disposal.  Off-site disposal methods
require sludge stabilization to produce an acceptable landfill
material.  On-site disposal in lined settling ponds was selected
for this study.

          Both the MgO and W-L/A processes produce an S02 stream
from regeneration of the S02 scrubbing liquor.   In the Wellman-
Lord/Allied process evaporator/crystallizers are used to regen-
erate the SOa scrubbing liquor.  For this study and in previous
commercial designs of the Wellman-Lord/Allied process,  single-
effect evaporators were used.   The use of a double-effect
evaporator would reduce the energy requirements for regeneration
by about 45 percent at the expense of increased capital costs
(OT-051).  Because the regeneration operation produces a
                              -18-

-------
concentrated (>90 percent) SO2 stream (OT-051),  conversion to
elemental sulfur or sulfuric acid is possible.  For this study,
a proprietary process of the Allied Chemical Company was selected
for converting the S02 to elemental sulfur.
                                                               r
          In the MgO process, oil-fired dryers and calciners are
used to decompose MgSOs into recycle MgO and a dilute (<10 per-
cent) SO2 stream.  Although the S02 can be converted into sulfur
or sulfuric acid, conversion to sulfuric acid was chosen because
the S02 stream also contains 5 to 10 percent 02  (OT-051, ZO-008).
The 02 is beneficial to the production of sulfuric acid, but it
increases the quantity of reducing gas required to produce ele-
mental sulfur.

3.2.2     Design Assumptions for Physical Coal Cleaning

          Several of the model S02 control systems selected by
the EPA for this study included examination of physical cleaning
of high sulfur eastern coals and then combusting the cleaned
coal using an FGD system.  This approach to utilizing coal clean-
ing as an S02 control technique is not commonly practiced in the
utility industry where economic considerations are of vital im-
portance.  Coal cleaning plants specifically designed for sulfur
removal generally produce three coal products.  One product has
a sulfur content low enough to be combusted, without using an
FGD process, in power plants which have to comply with the S02r
emission standard for new sources.  A second product fraction
with a slightly higher sulfur content can be.combusted without
S02 controls in plants which have to comply with the emission
standard for existing sources.  The third product fraction has
a very low heat content, and must be blended with raw coal or one
of the clean coal products.  Combustion of this blend will re-
quire flue gas desulfurization.  To conform with the emission
control systems defined by the EPA, the three .clean coal products

-------
 produced by a coal cleaning plant are assumed to be combined and
 combusted in one power plant.   The compositions  of the  physically
 cleaned eastern coals  and the  assumptions  used in calculating
 these compositions are shown in Table 3-4.

        TABLE 3-4.   COMPOSITIONS OF PHYSICALLY CLEANED COALS
                         Physically cleaned
                          3.5% sulfur  coal
Physically cleaned
 7.0% sulfur coal
Moisture, Ash Free
Coal, wt. %
Ash, wt. %
H20, wt. %
Sulfur, wt. %
Heating Value, MJ/kg

87.1
6.6
6.3
2.2
29.2

87.1
6.6
6.3
4.4
29.2
Assumptions

   50% ash removal
•  40% sulfur removal
   95% energy recovery efficiency  (RO-325)
   50% of product coal is thermally dried  (CH-307)
   heat for thermal dryer is supplied by combusting product coal

3.2.3     Design Assumptions for Coal Transportation

          The unit train is the most economic method for trans-
porting coal by rail over long distances on a continual basis.
There are several economic advantages of unit trains.  They em-
ploy specially designed hopper cars and locomotives.  Minimal
time loading and unloading is required, so equipment usage is
maximized.  The following assumptions were used in calculating
the energy requirements of the unit trains examined in this study:

          1)  Total one-way train distance between coal mine
              and power plant is 2,%100 km  (1300 miles).
                              -20'

-------
2)  Each unit train consists of 100 coal cars
    with a coal capacity of 91,000 kg  (100 ton)
    (WH-101).

3)  Each unit train uses 5 locomotives rated at
    2,700 kW-(3,600 HP) with the following diesel
    fuel oil consumption (WH-101, RA-215):

    •  At full power:  0.00021  m3/s  (200 gal/hr)
                       per locomotive
    •  At reduced power:  0.000029 m3/s  (28 gal/hr)
                          per locomotive

4)  Four hours each are required for  loading and
    unloading while the train moves at reduced
    power (BU-1,16, RA-215).

5)  One hour is required for passing  a large city
    and for undergoing each federal;inspection,
    while the train moves at reduced  power (BU-116,
    RA-215).

6)  One large city every 180 km (110 miles) and
    one federal inspection every 800 km (500 miles).

7)  Average train speed in open country is
    48 km/hr (30 mph) when loaded and 96 km/hr
    (60 mph) when empty (SO-138).

8)  One percent of the total train,load is lost
    as coal dust blow-off which occurs primarily
    during loading and unloading (CO-129).
                    -21-

-------
4.0
RESULTS
          The model power plant/S02  emission  control  systems
 selected by  the EPA for  examination  in  this study are shown in
 Table 4-1.   The systems  include  thirteen  control cases, which
 are grouped  under  three  emission control  levels.  Energy require-
 ments for the control  systems were calculated from the base case
 data and extrapolation methods described  in Appendices A through
 G.  In Section 4.1, these energy requirements are compared with
 respect 'to the techniques used to control SCh emission and with
 respect to the three S02 control levels.

          The energy requirements for the model control systems
 were also compared with  total U.S. energy demands in  1987 and
 1997.  Growth projections for the coal-fired  segment  of the
 electric power industry  and for  total U.S. energy consumption
 were obtained for  the  years 1987 and 1997.  The energy penalties
 imposed by the various SOa emission control systems were multi-
 plied by the projected capacities of the new  emission sources.
 The resulting total energy penalty data were  then compared to
 the total U.S. energy  demand.  Section 4.2 summarizes the results
 of these comparisons.
4.1
    Control Systems Comparisons
          A process operation breakdown of the energy require-
ments for each FGD process shows that energy requirements for
some of the operations depend on the amount of SOa removed and/or
degree of SOz removal.  There are six energy consuming operations
in the FGD processes:

              Raw material handling and feed preparation ,
              Particulate/chloride removal,
                             -22-

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               S02  scrubbing,
               Reheat,
               Fans, and
               Sulfur  recovery/disposal.

 The  energy requirements for  these  operations  are  listed  in
 Table  4-2  for  a 500 MW plant  using 3.5 and  7.0 percent sulfur
 coals.

        •   For  the  nonregenerable FGD processes—limestone, lime
 and  double-alkali--particulate/chloride scrubbers, reheaters,
 and  fans account for  65  to 90 percent of the  total system energy
 requirements.   The remaining  energy requirements  are for the S02
 scrubbers,  raw material  handling,  and feed preparation.  Minimal
 amounts are required  for calcium sulfite/sulfate  sludge disposal.
 Since  only the energy  requirements for these  latter three opera-
 tions  depend on the amount of S02  removed, the energy require-
ments  for  nonregenerable FGD processes are relatively insensitive
 to changes  in  coal sulfur content  and S02 removal level.

           For  the  regenerable FGD processes—magnesia slurry and
¥ellman-Lord/Allied—the sulfur recovery operations account for
a large majority of the  total system energy requirements (55 to
 65 percent  for the MgO process and 80 to 85 percent for the W-L/A
process).   Since the energy requirements of the sulfur recovery
operations  depend  directly on the amount of S02 removed from the
flue gas, the  total system energy requirements are strongly de-
pendent on  the  sulfur content of the coal and the S02 removal
level.
           It may be of  interest  to examine  the energy require-
                                                              s
ments of "bare bones" S02  control systems.  For the limestone
and lime FGD systems, this would entail deleting the energy re-
quirements associated with particulate/chloride removal and flue
gas reheat.  For the magnesia  slurry, W-L/A and double-alkali

                             -24-

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 "bare bones"  S02 control  systems to the control systems presented
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    TABLE 4-3.
COMPARISON OF TOTAL SYSTEM vs.  "BARE BONES"
   SYSTEM ENERGY REQUIREMENTS
Coal Sulfur
FGD Process • Content
Limestone
Lime
Magnesia Slurry
Wellman-Lord/
Allied
Double-Alkali
3.5%
7.0%
3.5%
7.0%
3.5%
7.0%
3.5%
7.0%
3.5%
7.0%
Total System Energy
Requirements,. MJ/s
49.2
57.3
44.3
48.2
77.5
124
176
321
39.8
40.7
"Bare Bones" System ' Percentage
Energy Requirements, MJ/s Difference
21.9
29.8
17.0
20.9
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156
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Assumptions
 500 MW power plant (net generating capacity)
 90% SOZ removal
 Uncontrolled power plant net heat rate = 2640 J/kW-s
 Steam produced in Magnesia Slurry and Wellman-Lord/Allied processes is used within
  the process.
 Magnesia Slurry process produces sulfuric acid as a by-product.
 Wellman-Lord/Allied process produces sulfur as a by-product.

           Estimates  of the energy requirements,  including the
energy required for  particulate/chloride removal  and flue gas
reheat, are listed in Tables  4-4  through 4-6.  The data in  these
tables  can be expressed in several  ways.  Two methods were  chosen
for  this study.  First, the energy  requirements were divided by
the  net electrical generating capacity of the power plant to
give J/s/kW or J/kW-s.   Expressing  the data in this manner  per-
mits  the data to be  extrapolated  to power plant capacities  other
than those  considered in this study.   For example,  a 400 MW
(400,000 k¥) power plant may have design and operating parameters,
                                -26-

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-------
including uncontrolled net plant heat rate, similar to one of
the 500 MW plants considered in this study.  The energy penalty
data for the 500 MW plant can then be multiplied by 400,000 kW
to determine the energy penalty for the 400 MW plant.

          The  second method of expressing  the energy penalty data
is as a percent of the energy input to an  uncontrolled plant with
the same net heat rate and net generating  capacity.  This method
identifies, for a given generating capacity, the percentage in-
crease in energy consumption resulting from control of S02 emis-
sions .
          An examination of the data in Tables 4-4 through 4-6
shows that on a per kilowatt or percentage basis, power plant
capacity has little influence on the energy requirements of the
emission control systems.  Therefore, it is only necessary to
look at one plant capacity to compare the different levels and
means of controlling S02 emissions.  Since 500 MW plants were
examined for all thirteen control cases, the data for this plant
capacity were selected for the comparative analyses.
4.1.1
Comparison by S02 Control Level
          Three S02 emission control levels were examined:
             0.52 g S02/MJ (1.2 Ib S02/106 B.tu) of heat
             input (the existing NSPS)
             90% SO2 removal by FGD
             0.22 g S02/MJ (0.5 Ib S02/106 Btu) of heat
             input
Comparisons of the energy requirements for the control systems
achieving these three control levels are presented in the follow-
ing sections.
                              -30-

-------
          0.52 g S02/MJ

          The energy requirements for the five cases which control
SO2 emissions to the existing NSPS of 0.52 g S02/MJ (1.2 Ib S02/
106 Btu) of heat input are shown in Figure 4-1.  In addition to
indicating the total energy penalties for the control cases, the
data in Figure 4-1 are separated into the type of energy required,
i.e., steam, electricity, natural gas or fuel oil for the FGD
process, diesel fuel oil for unit trains and coal losses from
physical coal cleaning or transporting coal.  The following ob-
servations can be made from the data in Figure 4-1:

             The smallest energy penalty is imposed by
             use of the nonregenerable FGD processes.

             The three nonregenerable FGD processes
             (limestone, lime and double-alkali) im-
             pose approximately equal energy penalties.
             The limestone process requires slightly
             more energy than the lime and double-alkali
             processes.

             Of the two regenerable FGD processes, the
             Wellman-Lord/Allied process requires over
             twice as much energy as the MgO process.

             Shipping low sulfur western coal to the
             Midwest requires from 25 to over 100 percent
             more energy than burning a high sulfur coal
             and using a nonregenerable FGD process.

             Phyically cleaning coal prior to combustion
             and also using the limestone or, lime FGD
                               -31-

-------

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                  3.6% SULFUR.
                  27,9Mjyfca
                   COAL
               7.0%SULFUR.   0.6 % SULFUR.  0.8% SULFUR.  3.5% SULFUR.

               27.9 M J/cg   20.9MJ/kg  25.6 MJ/kg   27.9 M J/kg
                COAL      COAL     COAL      COAL
Figure 4-1,
Energy requirements  for  S02 and particulate
control  -  0.52  g S02/MJ  control level, 500 MW  plant
                                 -32-

-------
             process requires about three times the
             energy required when dnly the' FGto process
             is used.

          90% SO2 Removal by FGD

          The energy requirements for the four control cases
which achieve 90 percent SO 2 removal are shown in Figure 4-2.
As was true for the 0.52 g S02/MJ control level, use of any of
the nonregenerable FGD processes requires about the same amount
of energy and the nonregenerable FGD processes impose much less
of an energy penalty than the regenerable FGD processes.  With
respect to changes in the sulfur content of the coal, the energy
requirements of the nonregenerable FGD processes change very
little (about a 10 percent increase when the sulfur content of
the coal doubles from 3.5 to 7.0 percent).  However, the energy
requirements of the regenerable FGD processes show a strong de-
pendence on the sulfur content of the coal.   Doubling the coal
sulfur content from 3.5 to 7.0 percent increases the energy re-
quirements of the MgO process by about 50 percent and of the
Wellman-Lord/Allied process by about 100 percent.  This arises
because the S02 recovery operations represent 55 to 85 percent
of the energy required by these processes.

          0.22 g S02/MJ

          The energy requirements for the four cases which con-
trol S02 emission to 0.22 g S02/MJ (0.5 Ib S02/106 Btu) of heat
input are shown in Figure 4-3.  As for the other two control
levels, the energy requirements of the limestone and lime FGD
processes are essentially equal.  The two control cases which
include physical coal cleaning followed by use of the lime or
limestone FGD process again illustrate the significant energy
penalty associated with physical coal cleaning.
                               -33-

-------
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              27.0U.Ukg COAL
                                       0.8% SULFUR
                                              O.S% SULFUR
Figure 4-2.
Energy penalties for  S02 and particulate
control - 90% removal control level,
500  MW plant.
                               -34-

-------




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0.8% SULFUR, 0.8% SULFUR, 3.6% SULFUR,
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7.0% SULFUR.
27.9 MJ/kg
COAL
Figure 4-3.
Energy requirements for SO2 and particulate
control - 0.22 g.S02/MJ control level, 5.00 MW plant.
                            -35-

-------
 4.1.2
Comparison by Coal Used
           The energy requirements of the model S02 emission
 control systems are compared in this section with respect to the
 coal used.  These comparisons identify the different energy pen-
 alties incurred by complying with the three emission control
 levels.

           3.5% Sulfur Eastern Goal

           The emission control cases which use the 3.5 percent
 sulfur, 27.9 MJ/kg eastern coal are shown in Figure 4-4.   For
 the control cases which use only an FGD process for S02  control,
 the energy penalty for achieving 90 percent S02 removal  is only
 slightly higher (about 10 percent) than for complying with the
 existing NSPS of 0.52 g S02/MJ (1.2 lb S02/106  Btu) of heat
 input.   For the control cases which use physical coal cleaning
 in conjunction with the lime or limestone FGD process, there is
 essentially no difference in the energy penalties for complying
 with the existing NSPS or for reducing S02  emission to 0.22 g
 S02/MJ  (1.2 lb S02/106  Btu)  of heat input.   However, the  energy
 penalty for using coal cleaning with the lime or limestone FGD
 process is  almost three times the  energy penalty for  using the
 lime or limestone FGD  process as the only S02  control technique.

           7.0% Sulfur  Eastern Coal

          The  energy requirements  for  the three  control cases
which utilized  the  7.0  percent  sulfur  coal  are  shown  in Figure
4-5.  For the  limestone and  lime FGD processes  the  energy  pen-
alty for achieving  90 percent S02  removal is about  equal to  the
penalty for meeting the existing NSPS.  Physical  coal cleaning
followed by FGD requires over one  and one-half times  the energy
that is required by FGD alone.
                               -36-

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                    MgO FQD  W-L/A FOD   O-A FQO
Figure 4-4.  Energy requirements for SOa
             control -  3.57o sulfur coal,
                             and particulate
                             500 MW plant
               -37-

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Figure 4-5.
Energy requirements for S02  and particulate
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                           -38-

-------
          Low Sulfur Western Coals
          The energy requirements for the four control cases
which utilize the low sulfur western coals are shown in Figures
4-6 and 4-7.  The data in these figures show the very small dif-
ference in energy requirements for using the limestone or lime
FGD process to achieve either 90 percent SQz removal or 0.22 g
S02/MJ (0.5 Ib S02/106 Btu) of heat input.  This is expected due
to the similar properties of the two western coals.            !
4.2
Energy Penalty Projections
          The following projections of new coal-fired electric
generating capacity which would be affected by a revised S02 new
source performance standard were supplied by the EPA:
                               New Coal-Fired Generating Capacity
          1983 through 1987                  65,000 MW
          1983 through 1997                 316,000 MW

The EPA also indicated that the average annual operating factor
for this new capacity would be 65 percent.  The energy penalty
data presented previously were used with these capacity projec-
tions to estimate the future effect of a revised NSPS on the
energy penalties of S02 emission controls.  It was assumed for
these calculations that the new capacity would be installed in
the form of 500 MW power plants.  However, the mix of coal feeds
and S02 control methods for these new plants and future S02 emis-
sion standards were not known.  In order to illustrate what the
minimum and maximum energy penalties may be, the projected new
generating capacities were multiplied by the energy requirements
for each of the 500 MW model power plant/S02 control systems.
These estimated energy penalties for 1987 and 1997 are listed in
Table 4-7 and 4-8, respectively.
                              -39-

-------
             <  160
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                           LEGEND: mi STEAM AND ELECTRICITY
                            i
                        LIMESTONE FGD
                                      i  !
i
Figure  4-6.  Energy requirements for  S02  and particulate
              control - low  heating value  Western  coal.
              500  MW plant.
                              -40-

-------
                            STEAM AND ELECTRICITY
         i
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                    LIMESTONE FQD
Figure 4-7.
Energy requirements  for SOz and particulate
control - high  heating value Western coal
500 MW plant.
                            -41-

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           While the open literature contains many  projections  of
 future  U.S.  energy demands,  these  projections  vary considerably.
 The  following  data are an average  of several projections  (BA-538)
           1987
           1997
Projected U.S.  Energy Consumption
  110 x 1018 J (100 x 1015 Btu)
  130 x 1018 J (120 x 1015 Btu)
These projections were used  to  calculate  the  "percent of Total
U.S. Energy  Consumption"  data shown  in Tables 4-7 and 4-8.

          The  data  in Tables 4-7 and 4-8  indicated that in 1987
controlling  S02 emissions  from  new sources, -i.e., those that come
on-line after  1982, would  increase U.S. energy consumption by an
estimated 0.1  to 0.8 percent.   In 1997 the increase in U.S. energy
consumption  is estimated  to be  0.4 to 3.4 percent.  The lower end
of these ranges represents use  of the nonregenerable FGD processes.
The high end of the ranges represents combustion of 7 percent
sulfur coal  and removing  90 percent  of the S02 by the Wellman-Lord/
Allied FGD process.  At the present  time  the limestone and lime
are the most widely used FGD processes.  This trend is anticipated
to continue  through 1997.  Therefore, estimates of 0.1 percent and
0.4 percent  for 1987 and 1997,  respectively,  are probably more
accurate.  For a given means of controlling S02 emissions, the
data indicated that to achieve  90 percent S02 removal requires
about 10 percent more energy than is required to meet the existing
NSPS.

          The S02 emission controls would also derate the projected
65,000 MW of new generating capacity installed in 1983-1987 by an
estimated 2,300 MW.  The projected 316,000 MW of new generating
capacity installed in 1983-1997 would be derated by an estimated
11,000 MW.
                              -44-

-------
                         REFERENCES

BA-538    Balzhiser, Richard E., "Energy options to the year
          2000", Chem. Eng. 73  (1977) Jan. 3, p. 74.  ..

BU-116    Buck, P. and N. Savage, "Determine Unit - Train
          Requirements", Power 118(1),  90 (1974) pp. 90-91.

CH-307    Choi, P. S., et-al., S02 reduction in non-utility
          combustion sources — technical and economic comparison
          of alternatives, final report.  EPA 600/2-75-073,
          Contract No. 68-02-1323, Task 13.   Columbus, Ohio:
          Battelle-Columbus Laboratories, Oct. 1974, .pp. 76, 77.

CO-129    Council on Environmental Quality,  Energy & The
          Environment; Electric Power.   Washington, B.C.,
          1973, p. 40.                              :

CO-380    "Coal Preparation and Unit-Train Loading", Coal Age
          1970  (July), pp. 188-202.

CO-644    Cooper, Tom, Private Communication, Combustion
          Engineering, September 23, 1977.

DE-064    Deurbrouck, A. ¥., Sulfur Reduction Potential of the
          Coals of the United States.  Report of Investigations
          7633.  Pittsburgh, PA.:  Pittsburgh Energy Research
          Center, 1972, pp. 16-19.

EN-587    Environmental Protection Agency, Office of Research
          and Development, Industrial Process Profiles:for
          Environmental Use, 26 volumes.  EPA 600/2-77-023 a-2,
          EPA Contract No. 68-02-1319,  Task 34.  Austin, TX.,
          Radian Corporation, various dates.  (Volume R, pp. 24-25)
                              -45-

-------
                    REFERENCES  (Continued)

FI-102    "Fine-Coal Treatment  and Water Handling", Coal Age  66
          (12), 67  (1961), p. 79.

KA-227    Kaplan, Norman, "Introduction to Double-Alkali Flue
          Gas Desulfurization Technology", Presented at the EPA
          Flue Gas  Desulfurization Symposium, New Orleans,
          Louisiana, March 1976, p. 411.

KO-174    Koehler,  George and James A. Burns, The Magnesia
          Scrubbing Process as Applied to an Oil-Fired Power
          Plant, Final Report.  EPA-600/2-75-057, EPA Contract
          No. EPA 70-114.  N.Y., Chemical Construction Corp.,
          October 1975, p. 4.

LO-071    Lowry, H.H. ed., Chemistry of Coal Utilization,
          2 vols. and supplementary volume.  N.Y., Wiley, 1945,
          1963 (Supplementary volume), pp. 325-331.

MC-136    McGlamery, G.G., et al., Detailed Cost Estimates for
          Advanced  Effluent Desulfurization Processes.
          Interagency Agreement EPA IAG-134 (D), Pt. A.
          Research  Triangle Park, N.C., Control Systems Lab.,
          NERC, 1974, pp. 13-17, 19-24, 30-68, 134-141.

OT-051    Ottmers,  D.M., Jr., et al., Evaluation of Regenerable
          Flue Gas Desulfurization Processes, revised report,
          2 vols., EPRI RP 535-1.  Austin, TX, Radian Corp.,
          July 1976, pp. 254, 320,  427-428.
                              -46-

-------
                    REFERENCES (Continued)

RA-215    Radian Corporation, A Western Regional Energy Develop-
          ment Study, 4 vols.  Final Report.   Radian Project No.
          100-064, PB 246264/6ST, PB 246265/3ST, PB 246266/1ST,
          PB 246267/9ST.  Austin, TX.,  August 1974.  Vol.  II,
          pp. 577, 578, 586.

RO-325    Robinson, Jerry, Private Communication, Battelle
          Research Corporation, 7 June 1977.

SA-311    Saleem, Abdus, Private Communication, Chemico,
          1 June 1977.

SO-138    Soo, S. L., et al. , The Coal Future, Appendix F, Coal
          Transportation, Unit Trains,  Slurry and Pneumatic
          Pipelines.  PB 248-652, NSF-RA-N-75-037-F.  Urbana,
          Illinois, University of Illinois at Urbana-Champaign,
          Center for Advanced Computation, June 1975, pp.  A6, A7.

WE-003    (Paul) Weir Company, An Economic Feasibility Study of
          Coal Desulfurization, 2 vols.  PB 176 845, PB 176 846.
          Chicago, IL, October 1965, Vol. I,  pp. 3-4.

WH-101    White, David Mills, An Analysis of Transportation
          Alternatives for Meeting Texas Industrial Demand of
          Western Coal Through the Year 2000.  Master's Thesis,
          University of Texas at Austin, August 1976, p. 43.

ZO-008    Zonis, Irwin S.,  et al., "The Production and Marketing
          of Sulfuric Acid  from the Magnesium Oxide Flue Gas
          Desulfurization Process", Presented at the Flue Gas
          Desulfurization Symposium, Atlanta, GA.,  November 1974,
          Essex Chemical Corp., 1974, p. 5.
                              -47-

-------
      APPENDIX A



LIMESTONE FGD PROCESS

-------
1.0
LIMESTONE FGD PROCESS
         The limestone flue gas desulfurization process uses
an aqueous slurry of limestone to absorb S02 from flue gases.
It is a nonregenerable desulfurization process since the S02
sorbent is continuously consumed, being discharged from the
process along with the absorbed S02 as a calciun? sulfite/sulfate
sludge.  Figure A-l is a simplified flow scheme of the limestone
FGD process selected for examination in this study.

         Flue gas from the power plant air preheater enters a
variable throat venturi scrubber.  Liquor injected into the
venturi removes approximately 99 percent of the flue gas parti-
culate matter and a small amount of S02.  Following particulate
removal, the flue gas enters a two-bed, mobile bed absorber.
Limestone slurry recirculated to this absorber can remove about
90 percent of the S02 present in the flue gas.  The overall chemis-
try of the SO 2 removal process can be represented by the follow-
ing two reactions:
CaC03
CaC03
S02
%02
                         CaS0
                                          C0
(1-D
(1-2)
 The flue gas exiting the S02 absorber is heated in an indirect
 steam reheater and compressed in an induced draft fan before
 entering the power plant stack for discharge to the atmosphere.

           A portion of the recirculating liquor in the particu-
 late scrubbing loop is directed to a lined settling pond where
 fly ash and calcium solids settle out.   Clarified pond water is
 returned to the S02 absorbers.  Makeup limestone slurry for the
 S02 absorbers is prepared on-site by crushing,  grinding and
 slurrying limestone.
                                A-2

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1.1
Base Case - Limestone FGD Process
         Material and energy balances were calculated for the
base case limestone FGD process - 90 percent removal of the SC-2
from the flue gas from a 500 MW power plant burning a 3.5 per-
cent sulfur coal.  The information used to prepare the material
balance (see Table A-l) and calculate energy requirements was
obtained from the open literature (MC-136).

         The limestone process consists of six basic processing
operations:
1.1.1
Raw material handling and preparation
Particulate scrubbing
SO2 scrubbing
Reheat
Fans
Calcium solids disposal

Raw Material Handling and Preparation
         The raw material handling and feed preparation processing
operation takes raw limestone and converts it into a slurry for
use as makeup reagent to the SOa absorbers.   Equipment in this area
includes storage bins, conveyors, crushers,  grinders, slurry
tanks, a dust collection system and pumps.  For the base case
design in which 6.30 kg/s (50,000 Ib/hr) of limestone (90 percent
CaCOs) are handled, the electric power requirements are estimated
at 790 kW.
                               A-,4

-------
TABLE A-l.  BASE  CASE MATERIAL BALANCE--LIMESTONE  FGD PROCESS
Stream
1
2

3

4

5
6
7
8

9
10
11
12
13
14
Stream
No. Description
Coal to Boiler
Combustion Air to
Boiler
Flue Gas to Air
Pr eh eater
Gas to Particulate
Scrubber
Gas to Reheater
Steam to Gas Reheater
Gas to I.D. Fans
Flue Gas to
Atmosphere
Slurry to Particulate
Scirubber
Makeup Water
Slurry to SO 2
Scrubber
Slurry to Settling
Pond
Makeup Limestone
Makeup Limestone
Rate
kg/s Nm3/s mVs Temperature, °K
47.3

570 430 317

555 421 647

611 464 428
637 518 325
8.88 517
637 518 346

637 518 353
1372 1.24
41.1 0.04
6048 5.8
69.0 0.06
6.3

        Slurry
10.0
0.006
                              A-5

-------
1.1.2
Particulate Scrubbing
          Included in the particulate scrubbing operation are
variable throat venturi scrubbers, effluent hold tanks with
agitators and scrubbing liquor recirculation pumps.  To achieve
approximately 99 percent removal of the flue gas particulate
matter, the venturi scrubbers are operated at a liquid to gas
ratio  (based on exit flue gas conditions) of 2 m3/1000 m3 (15
gal/1000 acf).  The electric power requirements for the re-
circulation pumps and agitators are estimated to be 920 kW.
1.1.3
SO2 Scrubbing
          The S02 absorbers selected for the limestone FGD pro-
cess are mobile bed absorbers.  Hold tanks with agitators and
scrubbing liquor recirculation pumps are also required.  To
effect 90 percent S02 removal in the base case design, a liquid
to gas ratio (based on exit flue gas conditions) of approximately
9.3 m3/100'0 m3 (70 gal/1000 acf) is required.  The electric
power requirements for S02 scrubbing are estimated to be 3,220
kW.                                         !
1.1.4
Reheat
          Scrubbed flue gas from a wet scrubbing process is
normally reheated to obtain a stack exit temperature of about
353°K (175°F).  This can be achieved by combustion of an auxil-
iary fuel with direct injection of the hot combustion gases into
the scrubbed flue gas or by indirect heating with steam.  The
latter method was selected because the reheat steam can be ob-
tained from the power plant boiler.  Since some reheat is pro-
vided by the induced draft fans downstream of the reheater,
                              A-6

-------
approximately 21°K (38°F) of additional reheat are required.
For the base base, the reheat energy requirements are estimated
to be 15.6 MJ/s (53.2 x 106 Btu/hr).   At an available steam heat
content of 1.75 MJ/kg (755 Btu/lb), the steam requirements for
the reheater are 8.88 kg/s (70,400 Ib/hr).
1.1.5
Fans
          Induced draft fans located downstream of the flue gas
reheater are used to overcome the pressure drop of the flue gas
as it passes through the limestone FGD process.  For the base case
design, which has a pressure drop of 6.5 kPa (26 in. H20),  the
electric power requirements for the fans are estimated to be
6,150 kW.
1.1.6
Calcium Solids Disposal
           This  process  operation  includes  a  pond  feed  tank with
agitator, a lined settling pond and pumps for transporting the
fly ash/calcium solids slurry to the settling pond and returning
pond water to the scrubbing system.  Since the calcium solids
represent about 60 percent of the total solids directed to the
settling pond, the energy requirements for solids disposal are
prorated using this factor.  For the base case design in which
2.58 kg/s  (10.3 ton/hr) of SOa are removed, the electric power
requirements for disposal of the resulting calcium solid are
estimated at 100 kW.
1.1.7
Utilities and Services
          Utilities and services such as instrument air,
lighting, heating, cooling, etc., are required for the limestone
FGD facilities.  For the base case design, the electric power
requirements for utilities and services are estimated at 60 kW.
                              A-7

-------
1.1.8
Base Case Summary
          The electricity and steam requirements for the base
case limestone FGD process are summarized in Table A-2.  As
shown by the data in this table, a 500 MW power plant burning
a 3.5 percent sulfur coal without any S02 emission controls
would require an energy input of 1.32 GJ/s (4.50 x 109 Btu/hr).
Reducing the S02 emissions from this plant by 90 percent with
a limestone FGD system would derate the power plant by 18 MW.
This assumes that all of the energy requirements of the FGD
system are obtained from the power plant.  The uncontrolled
plant net heat rate is 2,640 J/kW-s (9,000 Btu/kW-hr).  Since
the net heat rate for the controlled plant is 2,740 J/kW-s
(9,350 Btu/kW-hr),  the energy penalty of the'S02 control system
is 100 J/kW-s (350 Btu/kW-hr).

          A percentage breakdown of the energy requirements for
the base case limestone FGD process are shown below.

          Raw material handling and preparation - 4%
          Particulate scrubbing                 - 5%
          S02 scrubbing                         -18%
          Reheat                                -37%
          Fans            .                      -34%
          Calcium solids disposal               -<1%
          Utilities and services                -<1%

The particulate scrubbers, reheaters and fans account for about
75 percent of the base case limestone system energy requirements.
Since the energy requirements for these process operations depend
essentially only on the flue gas flow rate, a very large portion
of the total system energy requirements are insensitive to the
S02 concentration in the flue gas.  This indicates that for a
given power plant capacity,  the energy requirements for the S02
                               A-8

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emission control systems which use the limestone FGD process should
be approximately equal.  Differences which do occur result from
the dependence of the raw material handling and preparation and
S02 scrubbing operations on flue gas S02 concentration and S02
r emoval 1eve1.
1.2
Base Case Extrapolation
          The electricity and steam requirements for all of the
S02 control cases which use the limestone FGD process can be ex-
trapolated from the base case data.  The electric power require-
ments for the raw material handling and preparation, and calcium
solids disposal operations am proportional to the amount of S02
removed.  For particulate scrubbing, reheat, and utilities and
services, the electric power and steam requirements can be related
to the flue gas flow rate exiting the power plant air preheater.
The following extrapolation factors were identified for these
five segments of the limestone FGD process:
Raw material handling and preparation
Particulate scrubbing
Reheat
Calcium solids disposal
Utilities and services
                              306 kW/(kg S02  rem./s)
                              1.98 kw/(Nm3/s)
                              33.5 kJ/Nm3
                              38.7 kW/(kg S02 rem./s)
                              0.13 kW/(Nm3/s)
          The electric power requirements for the S02 scrubbers
and fans are dependent on the S02 concentration in the flue gas
and the desired S02 removal level.  Methods of calculating the
power requirements for these operations are described below.

1.2.1     S02 Scrubbing

          Variables which determine the amount of S02 that can
                              A-10

-------
be  removed in a mobile bed absorber include:
         •  the liquid to gas ratio,
         •  the gas  velocity,
         •  the scrubbing liquor pH,
         •  the inlet S02 concentration,
         •  the height of the bed,  number of beds,  and
           diameter of packing,  and
         •  the chloride and magnesium ion concentration
           in  the scrubbing liquor.

Based on test data for limestone  wet scrubbing using a turbulent
•bed contactor (a type of mobile bed) at the TVA Shawnee plant,
Bechtel  Corporation developed the following semi-empirical cor-
relation relating  the above variables to S02 removal.
T1 S02 = 1 - exp[-2.05 x 10 "* x (L/G)
                               0 • 81    0 • 36
                                    x v    exp[4.3 x 10~3 x v x (h/d + N)
+ 0.81 x pH± + 7.9 x 10 5 x (Mg) - 1.7
                                   x
                                                      ~5
                                         x Y± + 1.3 x 10~  x (Cl)]]   (1-3)
          where
                   nS02
                   L/G

                   v
                   h
                   d
                   N
                        = fraction of S02 removal
                   Y
                   Cl

                   Mg
                          liquid to gas ratio
                          outlet conditions
                                             gal/1000 cf at
                          gas velocity, ft/s
                          height of bed, in
                          diameter of packing, in
                          number of beds
                          inlet scrubbing liquor pH
                          inlet S02 concentration, ppm
                          inlet scrubbing liquor chloride
                          concentration, ppm
                          effective inlet scrubbing liquor
                          magnesium concentration, ppm
                               A-11

-------
          The following values, which  are  typical  of  those  used
in the development of the Bechtel correlation, were assumed for
use in Equation  (1-3) :.
V
h
d
N
•PH±
Cl
Mg
= 10 ft/s
= 15 in.
= 1.5 in .
= 2
= 6.0
= 3,000 ppm
= 0 ppm
Substituting these values into Equation (1-3) gives

        = 1 - exp[-4.7 x 10"" x (L/G) °'81 exp[5.4 - 1.7 x l(f * x Y ] ]   (1-4)

Equation 1-4 was developed  from  data which included inlet S02
concentrations of 1500-4500 ppm.  Although use  of low sulfur
western coals produces  inlet S02 concentrations of about 500
ppm, it is  felt that Equation 1-4 will  give reasonable estimates
of L/G's for  these  inlet  S02 concentrations. Since the power
requirements  for S02 scrubbing are  directly related to the
scrubbing liquor flow rate,  knowledge of  the required L/G and
the flue gas  flow rate  permits calculation of the electric power
requirements.  Table A-3  lists the  L/G's  calculated from Equa-
tion (1-4).
1.2.2
Fans
          Flue gas  flow  rate  and pressure  drop  are the two major
variables which affect the-energy requirements  of fans.   For the
                              A-12

-------
low pressure drops which fans must overcome, the following
equation can be used to calculate power requirements:
                   power required, kW =
                                          Q x AP
(1-5)
where     Q » flue gas flow rate, m3/s
         AP = pressure drop, kPa
          e = 0.690 = energy conversion efficiency of
                      fan and motor
Table A-3 lists the system pressure drops for the control cases
examined.  These pressure drops were calculated from the base
case data and a relationship developed by Bechtel for the
dependence of pressure drop on L/G in a turbulent contact
absorber.
                               A-13

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-------
   APPENDIX B



LIME FGD PROCESS

-------
1.0
LIME FGD PROCESS
          The lime flue gas desulfurization process is very simi-
lar to the limestone FGD process.  The major difference is the
source of alkalinity used to absorb SOz.   As the name of the
systems imply, the lime process uses a lime slurry while the
limestone process uses a limestone slurry.  The overall chemistry
of the lime process can be represented by the following reac-
tions .
          CaO + S02 -> CaS03
          CaS03 + %02 -*•
                                           (1-1)
                                           (1-2)
Figure B-l is a simplified flow scheme of the lime FGD process
s.elected for examination in this study.
1.1
Base Case - Lime FGD Process
          Material and energy balances were calculated for the
base case lime FGD process--90 percent removal of the SOa from
the flue gas from a 500 MW power plant burning a 3.5 percent
sulfur coal.  The information used to prepare the material
balance (see Table B-l) and calculate energy requirements was
obtained from the open literature_(MC-136)•

          There are six general process operations in the lime
FGD process:

             Raw material handling and preparation
             Particulate scrubbing
             SO2 scrubbing
             Reheat
             Fans
             Calcium solids disposal
                              B-2

-------
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-------
TABLE B-l.  BASE CASE MATERIAL BALANCE--LIME FGD PROCESS
Stream
1
2

3

4
5
6
7
8

9
10
11
12
13
14
Stream
No. Description
Coal to Boiler
Combustion Air to
Boiler
Flue Gas to Air
Preheater
Gas to Particulate
Scrubber
Gas to Reheater
Steam to Gas Reheater
Gas to I.D. Fans
Flue Gas to
Atmosphere,
Slurry to Particulate
Scrubber
Makeup Water
Slurry to SO 2
Scrubber
Slurry to Settling
Pond
Makeup Lime
Makeup Lime
Slurry
Rate
kg/s Nmd/s
47.3

570 430

555 421
611 464
637 518
8.88
637 518

637 518
1372
41.1
6048
69.0
2.9
25.3

mVs Temperature, °K


317

647
428
325
517
346

353
1.24
0.04
5.8
0.06

0.02
                           B-4

-------
The particxalate scrubbing and reheat operations are identical
to those in the limestone process.  Tor the base case design,
the electric power requirements for particulate scrubbing are
estimated to be 920 kW.  The steam requirements for the reheater
are estimated to be 8.88 kg/s (70,400 Ib/hr).
1.1.1
Raw Material Handling and Preparation
          The raw material handling and feed preparation opera-
tion is designed to receive pebble lime and prepare a 25 percent
solids slurry for use as makeup reagent for the SOa absorbers.
Major equipment items include conveyors, storage bins, vibrators,
slakers, a slurry surge tank and pumps.  For the base base
design in which 2.93 kg/s (23,200 Ib/hr) of lime (95 percent CaO)
are handled, the electric power requirements are estimated to
be 80 kW.
1.1.2
SO2 Scrubbing
          The S02 absorbers selected for the lime FGD process
are mobile bed absorbers.  Hold tanks with agitators and
scrubbing liquor recirculation pumps are also required.  To
effect 90 percent S02 removal in the base case design, a liquid
to gas ratio (based on exit flue gas conditions) of approxi-
mately 6.7 m3/1000 m3 (50 gal/1000 acf) is required.  The
electric power requirements for SOZ scrubbing are estimated to
be 2,300 kW.
1.1.3
Fans
          Induced draft fans located downstream of the reheater
are used to overcome the pressure drop of the flue gas as it
passes through the lime FGD process.  For the base case design
                              B-5

-------
which has a pressure drop of 6.4 kPa (26 in. H20),  the electric
power requirements for the fans are estimated to be 6,100 kW.
1.1.4
Calcium Solids Disposal
          The calcium solids produced in the S02 absorber are
disposed of in lined settling ponds.  For the base case design
in which 2.58 kg/s (10.3 ton/hr) of S02 are removed, the elec-
tric power requirements for disposal of the resulting calcium
solids are estimated to be 60 kW.
1.1.5
Utilities and Services
          The utilities and services required by the lime FGD
process are similar to those for the limestone process.   For
the base case design, the electric power requirements for utili-
ties and services are estimated to be 60 kW.
1.1.6
Base Case Summary
          The electricity and steam requirements for'the base
case lime FGD process are summarized in Table B-2.   As before,
a 500 MW power plant burning a 3.5 percent sulfur coal without
any S02 emission controls would require an energy input of 1.32
GJ/s (4.50 x 109 Btu/hr).  Reducing the S02 emissions  from this
plant by 90 percent with a lime FGD system would derate the
power plant by 16 MW.  This assumes that all energy requirements
of the FGD system are obtained from the power plant.  The un-
controlled plant net heat rate is 2,640 J/kW-s (9,000  Btu/kW-hr)
Since the net heat rate for the controlled plant is 2,730 J/kW-s
(9,320 Btu/kW-hr),  the energy penalty of the S02 control system
is 90 J/kW-s (320 Btu/kW-hr).
                              B-6

-------





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          A percentage breakdown of the energy requirements for
the base case lime FGD process are shown below:
Raw material handling and preparation -
Particulate scrubbing
S02 scrubbing
Reheat                                -
Fans
Calcium solids disposal
Utilities and services
                                                   6%
                                                  14%
                                                  41%
                                                  38%
The particulate scrubbers,  reheaters and fans account for about
80 percent of the lime system energy requirements.  Since the
energy requirements for these operations depend essentially
only on the flue gas flow rate, a very large portion of the
total system energy requirements are insensitive to the SO2  '
concentration in the flue gas.   This indicates that for a given
power plant capacity, the energy requirements for the S02
emission control systems which use the lime FGD process should
be approximately equal.  Differences which do occur result from
the dependence of the raw material handling and preparation and
S02 scrubbing operations on flue gas S02 concentration and S02
removal level.
1.2
Base Case Extrapolation
          The electricity and steam requirements for all of the
S02 control cases which use the lime FGD process can be extra-
polated from the base case data.  The electric power require-
ments for the raw material handling and preparation, and calcium
solids disposal operations are proportional to the amount of
S02 removed.  For particulate scrubbing, reheat, and utilities
and services, the electric power and steam requirements can be
                              B-8

-------
related  to  the  flue  gas  flow rate exiting the power plant air
preheater.  The following  extrapolation factors  were identified
for these five  segments  of the  lime FGD process:
          Raw material handling
          and preparation
          Particulate scrubbing
          Reheat
          Calcium solids disposal
          Utilities and services
                                 -30.9 kW/(kg S02 rem./s)
                                 -1.98 kW/(Nm3/s)
                                 - 33.5 kJ/Nm3
                                 -38.7 kW/(kg S02 rem./s)
                                 -0.13 kW/(Nm3/s)
          The power requirements  for  the  S02  scrubbers  and fans
are dependent on the S02 concentration  in the flue  gas  and the
desired S02 removal level.  Methods of  calculating  the  power
requirements for these operations  are described below.
1.2.1
        S02 Scrubbing
          Bechtel Corporation developed  an equation  for the
lime process that is similar in form  to  that used  for  calculating
L/G's for the S02 absorber in the  limestone process.
n
   S02
                     x (L/G)1'12 x v°*65 exp[0.0039 x v x (h/d + N)
+ 0.18 x pH± + 1.5 x lO"1" x (Mg) - 2.2 x 10 * x Y±]
                                                           (1-3)
   where
             nS02
             L/G

             v
             h
                = fraction of S02 removal
                = liquid to gas ratio, gal/1000 cf at
                  outlet conditions
                = gas velocity, ft/s
                = height of bed, in
                              B-9

-------
             d
             N
             pHi

             Yi
             Mg
               =  diameter  of  packing,  in
               =  number  of beds
               =  inlet scrubbing  liquor  pH
               =  inlet S02 concentration,  ppm
               =  effective inlet  scrubbing liquor
                  magnesium concentration,  ppm
          The following values which are  typical  of those used
in the development of the Bechtel  correlation, were assumed for
use in Equation  (1-3):

             v    = 12.5 ft/s
             h    =15 in.
             d    = 1.5 in.
             N    = 2
             pH±  =8.0
             Cl   = 3,000 ppm
             Mg   =0 ppm

Substituting these values into Equation  (1-3) gives
'S02
       = 1 - exp[-5.2 x 10~3 x (L/G)1*12 exp[2.0 - 2.2 x 10 * x Y±]]   (1-4)
Equation 1-4 was developed from data which included  inlet  S02
concentrations of 2000-4000 ppm.  Although some coals used in
this study produce inlet S02 concentrations outside  .this range,
it is felt that Equation 1-4 will give reasonable estimates of
L/G's for these inlet S02 concentrations.  Since the power
requirements for S02 scrubbing are directly related  to  the
scrubbing liquor flow rate, knowledge of the required L/G  and
                              B-10

-------
the flue gas flow rate permits calculation of the electric power
requirements.  Table B-3 lists the L/G's calculated from Equa-
tion (1-4).
1.2.2
Fans
          The equation for calculating the power requirements
for induced draft fans is given by Equation 1-5 in Appendix A.
The pressure drops for use in Equation 1-5 are given in Table
B-3 for the lime FGD control cases.
                              B-ll

-------
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-------
r
                                      APPENDIX C
                               MAGNESIA SLURRY FGD PROCESS

-------
1.0
MgO SLURRY FGD PROCESS
          The magnesia slurry (MgO) flue gas desulfurization
process uses an aqueous slurry of MgO to absorb S02 from flue
gases.  The process is termed regenerable since the scrubbing
slurry is thermal regenerated to produce MgO and S02.   The MgO
is recycled to the scrubbing system while the S02 is converted
into sulfuric acid.  Figure C-l is a simplified flow scheme of
the MgO slurry FGD process selected for examination in this
s tudy.

          Flue gas from the power plant air preheater first
enters a variable throat venturi scrubber.  A fly ash slurry is
injected into this venturi to remove particulates and chlorides,
The flue gas next enters a second venturi wherein S02  is ab-
sorbed by injection of magnesia slurry.  The overall chemistry
of the S02 absorption step can be represented by the following
reaction.
                       MgO + S02 -* MgS03
                                                (1-D
Flue gas exiting the second venturi is heated in an indirect
steam reheater and compressed in an induced draft fan prior to
entering the power plant stack for discharge to the atmosphere.
          A portion of the recirculating S02 absorber scrubbing
liquor is continuously removed and directed to the regeneration
facilities.  Here, MgS03 solids are separated from the liquor
and thermally regenerated in an oil-fired fluid bed calciner.
The calcination reaction is the reverse of Reaction 1-1.  The
regenerated MgO is recycled to the scrubber, while the S02 is
sent to a conventional contact sulfuric acid plant.  Makeup

-------
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magnesia slurry is prepared on-site by slurrying recycle and
fresh MgO.
1.1
Base Case-MgO FGD Process
          Material and energy balances were calculated for the
base case MgO FGD process - 90 percent removal of the S02 from
the flue gas from a 500 MW power plant burning a 3.5 percent
sulfur coal.  The information used to prepare the material
balance (see Table G-l) and calculate energy requirements was
obtained from the open literature (MC-136).
process:
1.1.1
          There are nine general operations in the MgO FGD
   Raw material handling and preparation
   Particulate/Chloride Removal
   S02 scrubbing
   Reheat
   F.ans
   Slurry processing
   Cake drying
   MgS03 calcining
•   Sulfuric acid production

Raw Material Handling and Preparation
          The raw material handling and feed preparation opera-
tion includes equipment for receiving coke and fresh MgO and
for storing, conveying and slurrying fresh and recycle MgO.
The equipment is designed to handle 0.038 kg/s (300 Ib/hr)  of
fresh MgO (98% purity), 2.09 kg/s (16,600 Ib/hr)  of recycle MgO
                              C-4

-------
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and 0.0275 kg/s (218 Ib/hr) of coke.  Based on these flow rates,
the electric power requirements are estimated to by 180 kW.
1.1.2
Particulate/Chloride Removal
          Included in the particulate/chloride scrubbing operation
are variable throat venturi scrubbers, effluent surge tanks and
recirculating slurry, makeup water and slurry disposal pumps.
The venturi scrubbers operate at a gas phase pressure drop of
2.1 kPa (8.5 in. H20) and a liquid to gas ratio (based on exit
flue gas conditions) of 2 m3/1000 m3 (15 gal/1000 acf).   For
the base case design, the electric power requirements for par-
ticulate scrubbing are estimated to be 1,090 kW.
1.1.3
SO, Scrubbing
          The S02 scrubbing operation includes variable throat
venturi scrubbers and magnesia slurry recirculation pumps.  The
scrubbers operate at an L/G (based on exit flue gas conditions)
of 2.7 mVlOOO m3 (20 gal/1000 acf) and a gas phase pressure
drop of 1.1 kPa (4.5 in. H20).   For the base case MgO process,
the electric power requirements for the. S02 scrubbing operation
are estimated to be 910 kW.
1.1.4
Reheat
          As for the limestone and lime FGD processes, indirect
steam reheaters are used to heat the scrubbed flue gas prior to
discharge to the atmosphere.  For the base case design which
requires approximately 18°K (33°F) of reheat, the reheater heat
duty is estimated at 13.9 MJ/s (47.4 x 106 Btu/hr).   A portion
of this heat duty, 0.85 MJ/s (2.9 x 106 Btu/hr), is  assumed to
be provided by steam generated in the MgS03 calcining area.
                              C-6

-------
Thus, the power plant boiler must provide only 13.0 MJ/s (44.5
Btu/hr).   At an available steam heat content of 1.75 MJ/kg
(755 Btu/lb),  the steam rate to the reheater is 7.44 kg/s
(59,000 Ib/hr).
1.1.5
Fans
          To overcome the pressure drop of the flue gas as it
passes, through the MgO FGD process, induced draft fans are lo-
cated downstream of the flue gas reheater.  For the base case
design which has a pressure drop of 5.7 kPa (23 in. H20),  the
electric power requirements for the fans are estimated to be
5,420 kW.
1.1.6
Slurry Processing
          The slurry processing operation receives a slipstream
of the recirculating liquor from the S02 absorbers.  This liquor,
which contains MgS03«6H20 solids, is first screened to remove
some of the water and then heated indirectly by steam to convert
the MgS03-6H20 to MgS03'3H20.  The resulting slurry is centri-
fuged, with the centrifuge cake being sent to the cake drying
operation while the centrate is returned to the S02 absorbers.
Based on the removal of 2.58 kg/s (10.3 tons/hr) of S02, the
electric power requirements for the slurry processing operation
are estimated at 380 kW.  The heat requirements are obtained
from steam produced in the waste heat boiler in the MgS03 cal-
cination operation.
1.1.7
Cake Drying
          Included in the cake drying operation are an oil-fired
fluid bed dryer, an air blower, a cyclone, a fabric filter, an
                              C-7

-------
 induced  draft  fan,  conveyors, and a MgS03  storage  silo.  The
 centrifuge cake from  slurry processing  is  thermally  dried  in
 the  fluid bed  dryer by hot gases produced  from  the combustion of
 fuel oil.  The dryer  offgases are treated  for particulate  re-
 moval before being  discharged to the atmosphere through the
 power plant flue gas  stack.  For treating  the MgS03  produced by
 removing 2.58  kg/s  (10.3 ton/hr) of S02 , the electric power re-
 quirements for the  cake drying operation are estimated at  410
,k¥.  The heat  rate  for the fluid bed dryer is estimated at
 16.0 MJ/s (54.4 x 106 Btu/hr).  Based on use of No.  6 fuel oil
 with a heating value  of 41.5 GJ/m3 (149,000 Btu/gal), the  fuel
 oil requirements are  0.000384 m3/s (365 gal/hr).
1.1.8
MgS03 Calcining
          MgS03 from the cake drying operation is calcined in
an oil-fired fluid bed calciner to produce MgO for recycle to
the S02 scrubbers and S02 for sulfuric acid production.  Equip-
ment in the calcining operation include feeders for MgS03 and
coke, conveyor-elevators, an oil-fired fluid bed calciner, a
combustion air blower, a waste heat boiler, a fabric dust
filter and a recycle MgO storage silo.  For treating the MgS03
produced by removing 2.58 kg/s (10.3 ton/hr) of S02, the electric
power requirements for the calcining operation are estimated at
380 kW.  The heat rate for the fluid bed calciner is estimated
at 17.4 MJ/s (59.6 x 106 Btu/hr).  Based on use of No. 6 fuel
oil requirements are 0.000420 m3/s (400 gal/hr).  The waste heat
boiler produces the equivalent of 4.23 MJ/s (14.4 x 106 Btu/hr)
of steam.  3.38 MJ/s (11.5 x 106 Btu/hr) of this steam is sent
to the slurry processing operation, while the remaining 0.85
MJ/s (2.9 x 106 Btu/hr) is credited to the flue gas reheater
heat duty.
                               C-8

-------
1.1.9
Sulfuric Acid Production
          The sulfuric acid production operation in the. MgO FGD
process is a conventional contact sulfuric acid plant.  Based on
a capacity of about 4.20 kg/s (400 ton/day) of 98 percent sul-
furic acid, the electric power requirements for sulfuric acid
production are estimated to be 1260 kW.
1.1.10
Utilities and Services
          The utilities and services required by the. MgO FGD
process are similar to those for the limestone process.  For the
base case design, the electric power requirements for utilities
and services are estimated to be 140 kW.
1.1.11
Base Case Summary
          The electricity, steam, and fuel oil requirements for
the base case MgO FGD process are summarized in Table C-2.
As before a 500 MW power plant burning 3.5 percent sulfur coal
without any S02 emission controls would require an energy input
of 1.32 GJ/s (4.50 x 109 Btu/hr).  Reducing the S02 emissions
from this plant by 90 percent with a MgO FGD system would derate
the power plant by 16 MW.  This  assumes that all electricity
and steam requirements of the FGD system are obtained from the
power plant.  The uncontrolled plant net heat rate is 2640 J/kW-s
(9,000 Btu/kW-hr).  Since the net heat rate for the controlled
plant is 2730 J/kW-s (9310 Btu/kW-hr), the energy penalty of the
S02 control system is 90 J/kW-s  (310 Btu/kW-hr).  However, the
base case MgO process also requires 0.000804 m3/s  (765 gal/hr)
of fuel oil.  This is equivalent to 33.4 MJ/s (114 x 106 Btu/hr).
Based on the controlled plant capacity of 484,000 kW, the ad-
ditional energy penalty associated with the fuel oil requirements
                              C-9

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is 70 J/kW-s (240 Btu/kW-hr).   Therefore, the overall S02
system penalty is 160 J/kW-s (550 Btu/kW-hr).
                                                control
          A percentage breakdown of the energy requirements for
the base case MgO FGD process are show below.
          Raw material handling and preparation
          Particulate/chloride removal
          S02 scrubbing
          Reheat
          Fans
          Slurry processing
          Cake drying
          MgS03 calcining
          Sulfuric acid production
          Utilities and services
                                            4%
                                            3%
                                           20%
                                           19%
                                            1%
                                           23%
                                           25%
                                            4%
Particulate/chloride scrubbers, S02 scrubbers, reheaters,  and fans
account for almost 50 percent of the MgO system energy require-
ments.  The energy requirements for these operations depend es-
sentially only on flue gas flow rate.  The S02 recovery operations
slurry processing, cake drying, MgSO3 calcining and sulfuric
acid production - also account for about one-half of the total
system's energy requirements.  Since the energy requirements for
these operations are proportional to the amount of S02 removed,
the energy requirements of the MgO system will exhibit a strong
dependence on the amount of S02 removed.
1.2
Base Case Extrapolations - MgO FGD Process
          The electricity, fuel oil, and steam requirements for
the three control cases which use the MgO FGD process can be
extrapolated from the base case data.  The electric power and
                              C-ll

-------
 fuel oil requirements for the raw material handling and prepara-
 tion,  slurry processing,  cake drying,  MgSO3 calcining,  and sul-
 furic acid production operations are proportional to the amount
 of SO2 removed.   The electric power and steam requirements for
 particulate/chloride removal, the reheaters and utilities and
 services can be  related to the amount of flue gas exiting the
 power plant air  preheater.  The following extrapolation factors
 were identified  for these eight segments of the MgO FGD process.
   Raw material handling
     and preparation
   Particulate/chloride
     removal
   Reheat
   Slurry processing
   Cake drying
  MgSOs calcining


  Sulfuric acid production-
  Utilities and services
                   68.0 kW/(kg  S02 rem./s)
                    2.34 kW/(Nm3/s)
                   28.1 kJ/Nm3
                   146 kW/(kg SO2 rem./s)
                   157 kW/(kg SO2 rem./s)
                   0.000149 m3  oil/(kg  S02 rem./s)
                   145 kW/(kg S02 rem./s)
                   0.000162 m3  oil/(kg  S02 rem./s)
                   473 kW/(kg S02 rem./s)
                   0.310 kW/(Nm3/s)
          The electric power requirements for the S02 scrubbers
and the I.D. fans are dependent on the S02 concentration in the
flue gas and the desired S02 removal level.  The energy require-
ments for these two operations in the three control cases which
use the MgO FGD process are described below.
1.2.1
S02 Scrubbing
          The coal sulfur contents and desired S02 control levels
for the three control cases which utilize the MgO process are:
                              C-12

-------
    Coal Sulfur Content
            3.5%
            3.5% - base case
            7.0%
                          S02 Control Level
                     0.52 g S02/MJ of heat input
                     90% S02 removal
                     90% SO2 removal
For the first control case listed above, a venturi scrubber with
a gas phase pressure of 0.75 kPa (3 in. H20) (KO-174) and an
L/G of 2.7 m3/1000 m3 (20 gal/1000 acf) was selected.  The elec-
tric power requirements for this scrubber used in a 500 MW power
plant are estimated to be 910 kW.  The second control case is
the base case and as mentioned previously, the electric power
requirements for S02 scrubbing are also established at 910 kW.

          To remove 90 percent of the S02 produced by combustion
of a 7.0 percent sulfur coal requires two contacting stages
(SA-311).   Therefore, for this case, a spray tower system
integral to a venturi scrubber was selected as the S02 absorber.
The spray system and venturi each operate at an L/G of 2.7
m3/1000 m3 (20 gal/1000 acf) and have a total pressure drop of
1.6 kPa (6.5 in. H20).  For this S02 absorber used in a 500 MW
power plant the electric power requirements for S02 scrubbing
are estimated to be 1820 kW.
1.2.2
Fans
          The equation for calculating the power requirements
for induced draft fans is given in Equation 1-5 in Appendix A.
The pressure drops for use in this equation are shown, below for
the three control cases which use the MgO process.
                              C-13

-------
    Coal
3.5% sulfur
3.5% sulfur
7.0% sulfur
     S02 Control Level
0.52 g S02/MJ of heat input
     90% removal
     90% removal
A'P kPa (in. H?0)
 6.22    (25)
 5.73    (23)
 5.35    (21.5)
                              C-14

-------
          APPENDIX D



WELLMAN-LORD/ALLIED FGD PROCESS

-------
1.0
WELLMAN-LORD/ALLIED FGD PROCESS
          The Wellman-Lord/Allied  (W-L/A) flue gas desulfuriza-
tion process is an aqueous, regenerable S02 control process.
A solution of sodium sulfite is used to absorb S02 from the flue
gas.  The scrubbing liquor is thermally regenerated to produce
an S02 stream which is then converted into elemental sulfur.
Figure D-l is a simplified flow scheme of the W-L/A process
selected for examination in this study.

          Flue gas from the power plant air preheater enters a
variable throat venturi scrubber.  A fly ash slurry is injected
into this venturi to remove particulates and chlorides.  The
flue gas next enters a three-plate valve-tray absorber.  S02 is
absorbed by a soultion of sodium sulfite which is recirculated
over each plate.  The overall chemistry of the S02 absorption
step can be represented by the following reaction:
Na2S03 + H20
               S0
                               2NaHS0
(1-1)
The desulfurized flue gas is heated in an indirect steam reheater
and compressed in an induced draft fan prior to entering the
power plant stack for discharge to the atmosphere.

          A portion of the recirculating S02 scrubbing solution
is continuously removed and directed to the regeneration facili-
ties.  Here, the solution is cooled to crystallize any Na2SO,t
formed by oxidation of sulfite in the absorber.  The NA2S0lf  is
then separated, dried and recovered as a solid by-product.   The
liquid separated from the Na2S01( is sent to an evaporator/
crystallizer wherein the reverse of Reaction 1-1 takes place.
The S02 liberated serves as the feed to the Allied Chemical sul-
fur recovery process.   A solution of soda ash and antioxidant
                             D-2

-------
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-------
 are prepared on-site,  mixed with the Na2S03  crystals  recovered
 from the evaporator/crystallizer and recycled to  the  S02
 absorbers.
 1.1
Base Case - Wellman-Lord/Allied FGD Process
           Material  and energy  balances were  calculated for  the
 base  case  W-L/A FGD process--90 percent  removal  of  the S02  from
 the flue gas  from a 500 MW power plant burning a 3.5 percent
 sulfur  coal.   The information  used  in preparing  the material
 balance (see  Table  D-l) and  in calculating energy requirements
 was obtained  from the  open literature  (MC-136).

           There are eight  general process operations within
 the W-L/A  FGD process.

              Raw material  handling  and feed preparation
           •   Particulate/chloride removal
              SO2  scrubbing
              Reheat
              Fans
              Purge  treatment
              SO2  regeneration
              SO2  reduction

 1.1.1     Raw Material Handling and Preparation

          Included  in the  raw material handling and feed pre-
paration operation  are equipment for receiving and storing soda
ash and antioxidant, and producing a mixture of these chemi-
cals for use as makeup reagent to the S02 absorbers.  Based on
handling 0.344 kg/s   (2650 Ib/hr) of soda ash (99.8% Na2C03)
and 5.71 g/s  (45.3 Ib/hr)  of antioxidant, the electric power
requirements are estimated to be 60 kW.
                             D-4

-------
TABLE D-l.
BASE CASE MATERIAL BALANCE--
WELLMAN-LORD/ALLIED FGD PROCESS
Stream
Stream No. Description
1
2
3
4
5
6
7
8
9
10
11
12
13
14
15
16
Coal to Boiler
Combustion Air to
Boiler
Gas to Air
Preheater
Gas to Particulate
Scrubber
Gas to SO 2
Scrubber
Gas to Reheat er
Steam to Reheater,
Gas to I.D. Fan
Gas to Atmosphere
Slurry to Particulate
Scrubber
Liquor to Purge
Treatment
Liquor to Evaporator/
Crystallizer
Natural Gas
Elemental Sulfur
Reduction Unit
Tail Gas
Dryer Off Gas
Rate
kg/s NmVs m3/s
47.3
570 430
555 421
611 464
664 522
662 518
7.57
662 518
662 518
1231 1.20
11.7 0.009
19.7 0.015
0.42 0.50
1.18
2.98 2.43
23.7 18.2
Temperature, °K

317
647
428
326
326
517
346
353



367

950
383
                      D-5

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 1.1.2
garticulate/Chloride Removal
           Included  in  the  particulate/chloride  removal  operation
 are variable  throat venturi,  scrubbers,  effluent hold  tanks  and
 recirculating slurry,  makeup water  and  slurry disposal  pumps.
 The venturi scrubbers  operate at a  gas  phase pressure drop  of 2.1
 kPa (8.5 in H20) and an overall liquid  to gas ratio (based  on
 exit flue  gas  conditions)  of 2 m3/10003m  (15 gal/1000  acf).
 For the base  case design,  the electric  power requirements for
 the particulate scrubbing  operation are estimated to be 1020 kW.
1.1.3
S02 Scrubbing
          Included in the S02 scrubbing operation are three-
plate valve tray absorbers and scrubbing solution reciruclation
pumps for each absorber plate.  The absorbers operate at a
pressure drop of 2.5 kPa (10 in. H20) and, based on exit flue
gas conditions, a liquid to gas ratio for each plate of 0.4 m3/
1000 m3 (3 gal/1000 acf).  For the base case design, the electric
power requirements for S02 scrubbing are estimated to be 320 kW.
1.1.4
Reheat
          As for the other FGD processes,  indirect steam re-
heaters are used to heat the scrubbed flue gas prior to discharge
to the.,atmosphere.  For the base case design which requires
.approximately 20°K (36°F) of reheat, the rcheater heat duty is
estimated at 13.3 MJ/s (45.3 x 106 Btu/hr).  At an available
steam heat content of 1.75 MJ/kg (755 Btu/lb),  the steam rate
to the reheater is 7.57 kg/s (60,000 Ib/hr).
                             D-6

-------
1.1.5
Fans
          To overcome the pressure drop of the flue gas as it
passes through the W-L/A FGD process, induced draft fans are
located downstream of the flue gas reheater.  For the base case,
design which has a pressure drop of 6.6 kPa (26 in. H20),  the
electric power requirements for the fans are estimated to be
6200 kW.
1.1.6
Purge Treatment
          The purge treatment operation is designed to take a
slipstream of the S02 absorber effluent and treat it for removal
of sodium sulfate.  The following equipment items are required:

             Ethylene glycol refrigeration, system
             Chiller/ crystallizer tank with agitator
             Feed cooler
             Centrifuge
             Conveyors'
             Pump s
             Rotary dryer
             Fabric dust filter
             Induced draft fan
The purge stream is first cooled in the feed cooler and sent to
the cooler/crystallizer.  Na2S04 solids formed upon cooling are
next separated in a centrifuge.  The centrate is directed to the
SO 2 regeneration operation while the solids are dried in a
rotary dryer by air heated by an indirect stream/ air heater.
The dryer off-gases are treated for removal of entrained NazSO^
and then combined with the flue gas stream exiting the power
plant preheater.  The sodium sulfate by-product is sent to
storage.
                             D-7

-------
           For the base case design in which 2.58 kg/s (10.3 ton/hr)
 of S02 are removed from the flue gas, the electric power require-
 ments for purge treatment are estimated to be 930 kW.  The heat
 duty for the steam/air heater is 4.51 MJ/s (15.4 x 106  Btu/hr).
 However, 2.66 MJ/s (9.07 x 106 Btu/hr) of this is assumed to be
 provided by steam produced in the S02 reduction operation.   The
 heat duty that must be obtained from the power plant boiler is
 therefore 1.85 MJ/s (6.33 x 106 Btu/hr).  At an available steam
 heat content of 1.75 MJ/kg (755 Btu/lb), the steam requirements
 are 1.06 kg/s (8380 Ib/hr).
 1.1.7
SO2 Regeneration
           The SO2  regeneration operation includes  evaporator/
 crystallizers,  pumps,  condensers,  condensate strippers,  com-
 pressors  and dissolving  tanks.   The evaporator/crystallizers
 produce an overhead stream of S02  and H20 and a  concentrated
 slurry of NaaSOi*.   The H20 is removed from the overhead  stream
 by  cooling in water-cooled condensers.   The condensate is mixed
 with the  concentrated  NasSCK  slurry,  makeup soda ash  and anti-
 oxidant and recycled to  the S02  absorbers.   The  S02 is compressed
 and directed to the S02  reduction  operation.

           Based on removing 2.58 kg/s (10.3 ton/hr) of S02, the
 electric  power  requirements for  S02  regeneration are  estimated
 at  1670 kW.   The heat  requirements  are estimated at 79.1 MJ/s
271 x 106  Btu/hr).   Based on steam available from the  power
 plant  boiler with  a useful heat  content  of  1.75  MJ/kg (755 Btu/lb),
 the steam requirements are estimated  at  45.3  kg/s  (359,000 Ib/hr).
                             D-8

-------
1.1.8
SOZ Reduction
          The S02 reduction operation includes a complete unit
for the reduction of S02 to elemental sulfur.  The reduction oper-
ation is based on a proprietary process developed by Allied
Chemical.  The heart of the process is the catalytic reduction
of a major portion of the S02 to elemental sulfur and smaller
amounts of H2S.  The reductant is usually natural gas, although
the use of reducing gases containing CO arid H2 such as are avail-
able from refineries or the gasification of coal have been tested
The two predominate reduction reactions are
2S02
3S02
       2CH
                       .C02 4- 2H20 + 2S
                      -*• 2C02 + 2H20 + 2H2S
(1-2)
(1-3)
          The H2S produced from Reaction 1-3 and unreacted S02
are then converted to sulfur in a series of converter-condensers.
2H2S + S02 -*• 2H20
                              3S
                                             (1-4)
Since the three  sulfur  forming reactions  are  exothermic, a
significant amount of useful  energy  is recovered in waste heat
boilers.

          Based  on removing 2.58 kg/s  (10.3 ton/hr) of  S02,  the
electric power and natural gas requirements of  the S02  reduction
operation are estimated to be 320  kW and  0.573  m3/s  (72,800  scfh),
respectively.  This  operation produces a  steam  heat credit of
3.46 MJ/s  (11.8  x 106 Btu/hr) of which 0.804  MJ/s  (2.73 x 106
Btu/hr)  is used  within  the area for  maintaining the by-product
sulfur  in a liquid  state while in  storage.  The remaining
2.66 MJ/s  (9.07  x 106 Btu/hr) are  credited to the purge treat-
ment operation.
                             D-9

-------
  1.1.9
Utilities and Services
           The utilities and services required by the W-L/A FGD
 process are similar to those for other FGD processes.  For the
 base case design, the electric power requirements for utilities
 and services are estimated to be 70 kW.

 1.1.10    Base Case Summary

           The electricity,  steam and natural gas requirements
 for the base case W-L/A FGD process are summarized in Table D-2
 As before,   a 500 MW power plant burning a 3.5 percent sulfur
 coal without any S02 emission controls  would require an energy
 input of 1.32 GJ/s (4.50 x 10*  Btu/hr).   Reducing the S02
 emissions  by 90  percent  with a  W-L/A FGD system would derate
 the power  plant  by 51  MW.   This assumes  that  the electricity
 and steam  requirements of  the control system  are obtained  from
 the power plant.   The  uncontrolled  plant  net  heat rate  is  2640
 J/kW-s  (9000 Btu/kW-hr).  Since the net heat  rate for the
 controlled plant  is  2940 J/kW-s  (10,000 Btu/kW-hr),  the energy
 penalty  of the S02 control  system is  estimated at 300 J/kW-s
 (1080 Btu/kW-hr).

          The natural gas requirements of the control system are
 0.573 mVs (72,800 scfh).  This is  equal to 22.4 MJ/s (76 x 106
 Btu/hr) based on a natural gas energy content of 39.1 MJ m3
 (1050 Btu/scf).  Since the controlled power plant capacity is
 449,000 kW, the additional energy penalty associated with the
natural gas requirements is 50 J/kW-s (170 Btu/kW-hr).  There-
 fore, the overall S02 control system penalty is 350 J/kW-s
 (1190 Btu/kW-hr).
                             D-10

-------
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           A percentage breakdown of the energy requirements
 for the W-L/A FGD process are shown below.
                                                    2%
                                                    1%
                                                   10%
                                                   10%
                                                    3%
                                                   60%
                                                   15%
Raw material handling and preparation  -
Particulate/chloride removal
SO2 scrubbing
Reheat
Fans
Purge treatment
SO2 regeneration
SO2 reduction
Utilities and Services
 The S02  recovery operations—purge  treatment,  S02  regeneration and
 SO2 reduction--  account for about 80 percent of the total energy
 requirements  for the W-L/A process.  Since  the energy require-
 ments  for  these  operations are proportional to the amount of S02
 removed  from  the flue gas, the energy requirements of the whole
 process  will  also be a  strong function of the  amount of S02
 removed.
 1.2
Base Case Extrapolations - W-L/A FGD Process
          The electricity,. natural.gas and steam requirements
for the three control cases which use the W-L/A FGD process can
be extrapolated from the base case data.  For the raw material
handling and preparation, purge treatment, S02 regeneration and
SO2 reduction operations, the energy requirements are propor-
tional to the amount of S02 removed.  For the particulate/chloride
scrubbers, reheaters and utilities and services, the electric
power and steam requirements can be related to the flue gas
flow rate exiting the power plant air preheater.  The following
extrapolation factors were identified for these seven segments
of the W-L/A FGD process operations:
                             D-12

-------
          Raw material handling and
            preparation
          Particulate/chloride
            removal
          Reheat
          Purge treatment

          SO2 regeneration

          SO2 reduction

          Utilities  and  services
-24.8 k¥/(kg SO2 rem./s)

-2.20 kJ/(Nm3/s)
-28.6 kJ/(Nm3)
- 359 kW/(kg S02 rem./s)
  717 kJ/(kg S02 rem./s)
- 646 kW/(kg S02 rem./s)
  306 MJ/(kg SO2 rem./s)
- 114 kW/(kg SO2 rem./s)
0.221 m3CHif/(kg S02 rem./s)
0.15  kW/(Nm3/s)
          The L/G's  and pressure drops  for  the  S02  absorbers
are dependent on the flue gas S02 concentrations and
 the  desired S02  removal level.   However, in a  sodium based
 scrubbing system like the W-L/A process, S02 removal is  only
 minimally dependent on L/G and pressure drop.   Therefore, the
 base case L/G and system pressure drop were used for the three
 control cases which use the W-L/A process.   The electric power
 requirements for the S02 scrubber and  fans are then proportional
 to the flue gas  flow rate and the following extrapolation factors
 were used:

           SO2 Scrubbing - 0.69 k¥/(Nm3/s)
           Fans          - 13.4 k¥/(Nm3/s)
                              D-13

-------
        APPENDIX E



DOUBLE-ALKALI FGD PROCESS

-------
1.0
DOUBLE-ALKALI FGD PROCESS
          The double-alkali (D-A) flue gas desulfurization
process is essentially a hybrid process.  The S02 absorption
step utilizes a sodium based scrubbing liquor similar to that
used in the Wellman-Lord/Allied process.  Unlike the W-L/A
process which recovers elemental sulfur, the D-A process is a
nonregenerable process since the absorbed S02 is disposed of as
a calcium based sludge.  This portion of the D-A process is
similar to the lime FGD process.  Figure E-l is a simplified
flow scheme of the D-A FGD process selected for examination
in this study.

          Flue gas from the power plant air preheater first
enters a variable throat venturi scrubber,  A fly ash slurry is
injected into this venturi to remove particulates and chlorides.
The flue gas next enters a mobile bed absorber where the S02 is
absorbed by a recirculating solution of sodium sulfite.  The
overall chemistry of  the S02 absorption step can be represented
by the following reaction.
NA2S03 +  S02+H20
                                  2NaHS0
(1-D
The  scrubbed  flue  gas  is heated  in  an  indirect steam reheater
and  compressed in  an induced  draft  fan prior  to entering the
power plant stack  for  discharge  to  the atmosphere.

           The S02  absorber effluent is reacted with lime slurry,
causing calcium sulfite/sulfate  to  precipitate.  A portion  of
the  lime treated liquor is directed to a clarifier where soda
ash  is added  to reduce the amount of dissolved calcium in the
liquor and provide the necessary makeup  of sodium ions.  Calcium
solids are removed from the clarifier, and sent to a  lined  pond
for  disposal, while the clarifier overflow is returned to the
SO2  absorbers.
                             E-2

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1.1
Base Case - D-A FGD Process
          Material and energy balances were calculated for the
base case D-A FGD process-- 90 percent removal of the S02 from
the flue gas from a 500 MW power plant burning a 3.5 percent
sulfur coal.  The material balance for the base case D-A process
is given in Table E-l.

          There are six general process operations in the D-A
FGD process:

             Raw material handling and preparation,
             Particulate/chloride removal,
             SO2 scrubbing,
             Reheat,
             Fans, and
             Calcium solids disposal.
1.1.1
Raw Material Handling and Preparation
          The raw material handling and feed preparation opera-
tion includes equipment for receiving and storing soda ash and
pebble lime, and producing lime slurry and a solution of soda
ash.  The lime slurry is used to precipitate calcium sulfite
and calcium sulfate from the S02 scrubbing liquor.  The solution
of soda ash serves the dual purpose of softening the treated
SO2 scrubbing liquor and providing the required sodium ion
makeup.  Based on handling 0.214 kg/s (1700 Ib/hr) of soda
ash (99.8 percent Na2C03) and 2.26 kg/s (17,900 Ib/hr) of lime
(95 percent CaO), the electric power requirements for this opera-
tion are estimated to be 100 kW (MC-136).   The soda ash requirements
were calculated by assuming 0.05 mole of makeup soda ash were
required per mole of S02 removed, while the lime makeup was
based on stoichiometric requirements (KA-227).
                             E-4

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TABLE E-l.  BASE CASE MATERIAL BALANCE--DOUBLE-ALKALI FGD PROCESS
Stream No.
1
2
3
4
5
6
7
8
9
10
11
12
13
Stream
Description
Coal to Boiler
Combustion Air to
Boiler
Gas to Air
Preheater
Gas to Particulate
Scrubber
Gas to SO 2
Absorber
Gas to Reheat'er
Steam to Reheat er
Gas to I.D. Fan
Gas to Atmosphere
Slurry to
Particulate
Scrubbing
Slurry to S02
Absorber
Makeup Lime
Makeup Soda Ash
Rate
kg/s Nm3/s mVs
47.3
570 430
555 421 •
611. 464
635 500
637 518
8.88
637 518
637 518
1231 1.2
1568 1.2
2.9
0.21
Temperature, °K

317
647
428
326
325
517
346
"353




                              E-5

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1.1.2
Particulate/Chloride Removal
          The venturi scrubbers used for control of particulates
and chlorides in the D-A FGD process are essentially identical
to the venturi scrubbers used in the MgO process.  Based on an
L/G of 2 m3/1000 m3 (15 gal/1000 acf),  the electric power re-
quirements for particulate scrubbing are estimated to be 1090 kW
(MC-136).
1.1.3
SO2 Scrubbing
          Included in the S02 scrubbing operation are mobile bed
absorbers, scrubbing liquor hold tanks and liquor recirculation
pumps.  The S02 absorbers operate at an L/G of 2 m3/1000 m3
(15 gal/1000 scf) and a pressure drop of 2.1 kPa (8.5 in. H20).
For the base case design, the electric power requirements for
S02-scrubbing are estimated to be 860 kW (MC-136).
1.1.4
Reheat
          As for the other FGD processes, indirect steam reheat-
ers are used to heat the scrubbed flue gas prior to discharge
to the atmosphere.  For the base case design which requires
approximately 21°K (38°F) of reheat, the reheater heat duty is
estimated at 15.6 MJ/s (53.2 x 106 Btu/hr).   At an available
steam heat content of 1.75 MJ/kg (755 Btu/lb),  the steam rate
to the reheater is estimated at 8.88 kg/s (70,400 Ib/hr) (rC-136)
1.1.5
Fans
          To overcome the pressure drop of the flue gas as it
passes through the D-A FGD process, induced draft fans are
located downstream of the flue gas reheater.  For the base case
design which has a system pressure drop of 5.7 kPa (23 in. H20),
the electric power requirements for the fans are estimated to
be 5510 kW (MC-136).

                              E-6

-------
 1.1.6
 Calcium  Solids Disposal
           SO2  absorber effluent  which has  been treated with
 lime slurry is sent to clarifiers  for softening with  a solution
 of  soda ash.   The CaC03  solids formed here and the  CaS03  and
 CaSOit  solids formed by the  lime  treatment  are  removed from the
 bottom of  the  clarifier  and directed  to  centrifuges.  The solids
 from the centrifuges are washed  with  water and then combined
 with the effluent from the  particulate scrubbers for  disposal
 in  a lined settling pond.   Pond  water is recycled to  the  raw
 material handling and feed  preparation operation.  The clarifier
 overflow and centrifuge  wash are recycled  to the S02  absorbers.
 Based  on handling the solids formed by removing 2.58  kg/s
 (10.3  ton/hr)  of  S02,  the electric power requirements for cal-
 cium solids disposal are estimated at 250  kW (MC-136).
1.1.7
Utilities and Services
          The utilities and services required by the double-
alkali FGD process are similar to those for the limestone pro-
cess.  For the base case design, the electric power requirements
for utilities and services are estimated to be 60 kW (MC-136).
1.1.8
Base Case Summary
          The electricity and steam requirements for the base
case D-A FGD process are summarized in Table E-2.  As before,
a 500 MW power plant burning 3.5 percent sulfur coal without
any S02 emission controls would require an energy input of 1.32
GJ/s (4.50 x 109 Btu/hr).  Reducing the S02 emissions from this
plant by 90 percent with a D-A FGD system would derate the
power plant by 15 MW.  This assumes that all energy needs of
the FGD system are obtained from the power plant.  The
                             E-7

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 uncontrolled plant net heat rate is 2640 J/kW-s (9000 Btu/kW-hr)
 Since the net heat rate for the controlled plant is ,2720 J/kW-s
 (9280 Btu/kW-hr), the energy penalty of the SO2 control system
 is 80 J/kW-s (280 Btu/kW-hr).

           A percentage breakdown of the energy requirements for
 the base case D-A FGD process  are shown below.
Raw material handling and preparation  -
Particulate/chloride removal
SO 2 scrubbing
Reheat
Fans
Calcium solids disposal
Utilities and services
Particulate/chloride  scrubbers,  reheaters,  and fans account for
over  90 percent  of  the D-A  system energy requirements.  The en-
ergy  requirements for these areas depend essentially only on the
flue  gas flow rate.   Therefore,  the energy  requirements for the
D-A process will depend very little on inlet flue gas S02 con-
centration or SO2 removal level.
                                                    7%
                                                    6%
                                                   46%
                                                   38%
                                                    2%
1.2
Base Case Extrapolations
          The electricity and steam requirements for the three
control cases which use the D-A FGD process can be extrapolated
from the base case data.  The electric power requirements for the
raw material handling and preparation, and calcium solids disposal
operations are proportional to the amount of S02 removed.  For the
particulate/chloride scrubbers,  reheaters, and utilities and ser-
vices, the electric power and steam requirements can be related
to the flue gas flow rate exiting the power plant air preheater.
                              E-9

-------
The following extrapolation factors were identified for these
five segments of the D-A FGD process:
          Raw material handling and
             preparation
          Particulate/chloride
             removal
          Reheat
          Calcium solids disposal
          Utilities and services
  38.8  k¥/(kg  S02 rem./s)

   2.34 kW/(Nm3/s)

  33.5  kJ/Nm3
  95.6  kW/(kg  S02 rem./s)
   0.14 kW/(Nm3/s)
          While the L/G and pressure drop required by the SOz
absorbers are dependent on the flue gas SOz concentration and
the desired S02 removal level, this dependence in a sodium-based
scrubbing system like the double-alkali pricess is minimal.
Therefore, the base case L/G and system pressure drop were used
for the three control cases which use the D-A process.  The
electric power requirements for the S02 scrubbing and fans areas
are then proportional to the flue gas flow rate and the following
extrapolation factors were used:
          SO2 scrubbing
          Fans
-  1.84 kW/(Nm3/s)
- 11.9  kW/(Nm3/s)
                              E-10

-------
     APPENDIX F



PHYSICAL COAL CLEANING

-------
1.0
PHYSICAL COAL CLEANING
          Physical coal cleaning processes remove impurities from
coal via a mechanical separation process.  In most cleaning oper-
ations, this separation of impurities is based on a gravity dif-
ference between coal (which is relatively light) and contaminants
such as pyrite (FeS2),  ash, and rock (which are heavier) (WE-003) ,
Historically, ash and rock removal were the primary objectives
of coal cleaning.  However, the need for reducing sulfur dioxide
emissions has recently focused more attention on the sulfur re-
moval aspects of physical coal cleaning.

          Sulfur occurs in a coal seam in three basic forms:
pyritic, organic, and sulfate.  In any given coal the amount of
sulfate sulfur is negligible.  Physical coal cleaning is re-
stricted to removal of the pyritic sulfur from coal.  This  is
due to the fact that the organic sulfur in coal is chemically
bound and requires a chemical extraction process for removal.

          The effectiveness of a physical coal cleaning process
in removing  sulfur from coal is both coal and process specific
 (DE-064).  Data' related to the ability to physically clean  the
3.5 and  7,0  percent sulfur coals examined in this study were
not available.  Therefore, it was necessary to select a gener-
alized coal  cleaning plant.  Figure F-l  is a simplified flow
scheme of a  physical coal  cleaning facility depicting common
process  areas  (LO-071, CO-380).  The coal cleaning plant repre-
sented by this  flow scheme was selected  for this  study.

          The following four process areas are present  in  the
coal  cleaning facilities  shown in Figure F-l.  Listed under
each  area are various  operations which may be utilized  in  an
individual  cleaning process.
                                F-2

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1.1
   Initial Coal Preparation
   1)   Storage
   2)   Rough Cleaning/Primary Breaking
   3)   Raw Coal Sizing

   Fine Coal Processing
   1)   Wet Cleaning
   2)   Desliming

   Coarse Coal Processing

   Water Management/Refuse Disposal
   1)   Dewatering
   2)   Drying
   3)   Water Recovery
   4)   Refuse Disposal

Initial Coal Preparation
          Prior to the actual cleaning process, run-of-mine
(R.O.M.) coal must undergo initial preparation.  This involves
preliminary crushing of the coal to remove large rock fractions
and to liberate entrained impurities such as clay, rock, and
other inorganic materials including pyrite.  The first crushing
step is followed by a screening operation,, secondary crushing,
and a second screening step which produces two coal streams;
one containing a fine fraction (usually less than 6.5 mm) and
the other containing coarse particles  (nominally 76 x 6.5 mm).
These two coal streams are then fed to their respective process
areas where the actual cleaning operation takes place (CO-380,
LO-071).
                               F-4

-------
 1.2
 Fine  Coal  Processing'
           The process feed stream of less than 6,5 mm ooal is
 slurried with water as it enters the fine coal processing area.
 This slurry is then subjected to a desliming operation which
 removes a suspension containing approximately 50 percent of
 minus 200 mesh material (FI-102) .

           After desliming,  the oversize coal fraction (greater
 than 28 mesh)  is pumped to  the fine coal cleaning process.
 Here,  fine coal particles undergo  gravity separation in one of
 several wet cleaning devices.   This removes  a percentage of the
 ash and pyritic sulfur to produce  a clean coal product.   The
 product stream from this operation is  then fed to the drying
 area of the plant and refuse material  is further processed in
 the water treatment section.

           The  slimes removed from  the  fine coal are  fed to  a
 froth flotation process.  Upon entering the  flotation process
 area,  the slime suspension  is  treated  with a frothing agent
 which  selectively floats  coal  particles in the flotation mach-
 ines while allowing pyrite  and ash impurities  to settle.  The
 float  product  is  then sent  to  the  dewatering area while  reject
 material  is  processed in  the water treatment and recovery area.
1.3
Coarse Coal Processing
          Feed to the coarse coal processing area of the plant
consists of oversize material (76 x 6.5 mm particles) from the
initial preparation area.  This feed stream is slurried with
water prior to cleaning in one of the many types of process
equipment currently employed in coarse coal cleaning.  Here,
impurities are separated from the coal using differences in
                              F-5

-------
coal and reject densities.  It is also common practice to re-
move a middling fraction from the separation operation and fur-
ther process it by means of recycle or by feed to another
cleaning process.  These cleaning operations result in two
streams being removed from the coarse coal processing area:  a
product and reject stream.  After the coarse cleaning operation,
the product stream is pumped to the dewatcsring and drying area
of the plant while the reject stream is processed in the water
treatment and recovery area.
1.4
Water Management/Refuse Disposal
          Dewatering and drying equipment handle the product
flows from both the fine and coarse coal preparation areas.
Typically, cleaning plants employ mechanical dewatering oper-
ations to separate coal slurries into a low-moisture solid and
a clarified supernatant.  The solid coal sludge produced in the
dewatering step can then be mechanically or thermally dried to
further reduce the moisture while the supernatant from the de-
watering process  is returned to the plant's water circulation
system.

          The water treatment and recovery section of a cleaning
plant processes refuse slurries containing both coarse material
and reject slimes.  Here, the refuse slurry is dewatered in
thickeners and settling ponds.  The supernatant from this oper-
ation is returned for reuse in the plant while the refuse is
buried and revegetated to prevent spontaneous ignition.

          The coal product from the dewatering and drying area
of the plant can  be further processed.  This may involve crush-
ing and  screening operations to separate the product into vari-
ous product sizes.
                               F-6

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1.5
Physical' CcTaT 'Cleaning Design Premises
           As  mentioned previously,  the design of a physical
 coal  cleaning plant is dependent on the properties of the coal
 to  be cleaned.   However,  physical coal cleaning data were not
 available  for the 3.5  and 7.0 percent sulfur coals considered
 in  this  study.   In order  to  develop energy requirements  for
 the coal cleaning plant,  several assumptions had to be made.
 These assumptions are  discussed in  the following paragraphs.

           To  achieve sulfur  removal levels of about 40 percent
 would require a  fairly sophisticated cleaning plant.   In general,
 as  a  cleaning plant becomes  more sophisticated or complex,  its
 energy recovery  efficiency also increases.   Therefore, a 95
 percent  energy recovery--95  percent of the input coal energy
was recovered 'in  the clean coal  product—was  used (RO-325) .

           Other  assumptions  used in calculating the energy  re-
 quirements of a  coal cleaning plant were (CH-307):

           (1)  The  electric  power requirements  for  a
               278  kg/s (500  ton/hr)  cleaning  plant
               are  2980 kW.

           (2)  The  heat duty  of a thermal  dryer is
               534  kJ/kg  (230  Btu/lb)  of coal  dried.

           (3)  One  half of the  clean  coal product
               (the coal fines)  is  thermally dried.

           (4)  Heat for the thermal dryers is supplied
               by burning a portion of the clean coal
               product.
                            F-7

-------
          (5)  50% of  the  ash content of the coal
               is removed.

          (6)  The average heating value of the
               clean coal  is 29.2 MJ/kg (12,500 Btu/lb).

Based on ;these assumptions, the estimated compositions of  the
physically cleaned 3.5 and 7.0 percent sulfur coals are as
shown in Table F-l.  The energy requirements and throughput  for
physical coal cleaning plants supplying coal to 500 MW and 25 MW
power plants are  summarized in Table F-2.

          When assessing the energy penalty of the coal, cleaning
process, the electricity requirements are assumed to be obtained
from the power plant and are reflected in the power plant's  net
heat rate.  The penalty associated with the coal lost and  used
in the cleaning process are debited to the control system  by re-
quiring an increase  in the coal feed rate to the cleaning  plant.

     TABLE F-l.   COMPOSITIONS OF PHYSICALLY CLEANED COALS
                         Physically cleaned
                          3.5% sulfur coal
             Physically cleaned
              7.0% sulfur coal
     MAF Coal. wt.  %
     Ash, wt. %
     H20, wt. %
     Sulfur, wt. %
     Heating Value, MJ/kg
87.1
 6.6
 6.3
 2.2
29.2
87.1
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     APPENDIX G



COAL TRANSPORTATION

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1.0
GOAL TRANSPORTATION
          Unit trains are the major method used to transport
coal over long distances.  Unit trains are railroad systems
dedicated solely to the movement of coal from a coal mine or
coal preparation plant to an end user.  For this study, unit
trains are used to transport western coal from a mine in the
Four Corners area of New Mexico to a power plant in Ohio.  The
total one-way train distance between these two points is assumed
to be 2,100 km (1,300 miles).  The following assumptions were
used in calculating the energy requirements of a unit train:

          1)  Each unit train consists of 100 coal cars
              with a coal capacity of 91,000 kg (100 ton)
              (WH-101).

          2)  Each unit train uses 5 locomotives rated at
              2,700 k¥ (3,600 HP) with the following diesel
              fuel oil consumption (WH-101, RA-215):
                 At full power:

                 At reduced power:
                           0.00022 m3/s (200 gal/hr)
                           per locomotive
                           0.000029 m3/s (28 gal/hr)
                           per locomotive
          3)  Four hours each are required for loading and
              unloading while the train moves at reduced
              power (BU-116, RA-215).

          4)  One hour is required for passing a large city
              and for undergoing each federal inspection,
              while the train moves at reduced power (BU-116,
              RA-215).
                              G-2

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          5)  One large city every 180 km (110 miles)
              and one federal inspection every 800 km
              (500 miles).

          6)  Average train speed in open country is
              48 km/hr (30 mph) when loaded and 96 km/hr
              (60 mph) when empty (SO-138)..

          7)  One percent of the total train load is
              lost as coal dust blow-off which occurs
              primarily during loading and unloading
              (CO-129).

          8)  Diesel fuel oil has a heating value of
              38.4 GJ/m3  (138,000 Btu/gal).

Table G-l shows how these assumptions were used to calculate the
energy required to transport low sulfur western coal to a Midwest
power plant.  The energy penalties for the control systems which
examine transporting low sulfur western coal are given in Table
G-2.
                               G-3

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         TABLE G-l.   CALCULATION OF  ENERGY REQUIREMENTS
                       FOR TRANSPORTING WESTERN COAL
                Basis:  One round trip unit train delivery

# of hours at reduced power:
     Passing large cities  (24) - 24
     Undergoing federal        -  4
      inspection (4)
     Loading                  -  4
     Unloading                -  4
              Total           - 36 hrs.

# of hours at full power:
     En route to power plant   - 43
     Return to mine           - 22
              Total           - 65
     TOTAL duration of trip   - 101 hrs.
Fuel Consumption:
     @ reduced power
     @ full power
              Total
            Average
   734 GJ
 9,460 GJ
10,190 GJ
  28.0 MJ/s
Windage Losses,  Total  -
              Average  -
90,800 kg
  0.25 kg/s
Coal Transported,  MJ/kg coal
Average Fuel Consumption, MJ/s
Average Windage Losses, MJ/s
Total average Energy Consumed or Lost, MJ/s
Total average Energy Consumed or Lost, MJ/kg coal
J?.P_r
- 28.
- 5.
- 33.
- 1.
?....
0
2
2
33
25.6
28.0
6.4
34.4
1.38
                                   G-4

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        TABLE G-2.   ENERGY PENALTY --  COAL TRANSPORTATION
         Coal
Power Plant  Size
        MW
Coal Rate
  kg/s
 Transportation
 Energy Penalty
MJ/s      J/kW-s
0.4% Sulfur; 20.9 MJ/kg
0.4% Sulfur; 20.9 MJ/kg
0.6% Sulfur; 25.6 MJ/kg
0.6% Sulfur; 25.6 MJ/kg
        25
       500
        25
       500
  3.26
 63.0
  2.66
 51.6
 4.3
84
 3.7
71
170
170
150
140
                                   G-5

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TECHNICAL REPORT DATA
(Please read Instructions on the reverse before completing)
1. REPORT NO.
4. TITLE AND SUBTITLE
The Energy Requirements fen
from Coal-Fired Steam/Elecl
7. AUTHOR(S)
W. C. Thomas
9. PERFORMING ORGANIZATION NAME AN
Radian Corporation
P. 0. Box 9948
Austin, Texas 78766
2.
c Controlling S02 Emissions
trie Generators
?<

D ADDRESS
12. SPONSORING AGENCY NAME AND ADDRESS
Environmental Protection Agency
Office of Air Quality Planning and Standards (MD-13)
Research Triangle Park, North Carolina 27711
3. RECIPIENT'S ACCESSION-NO.
5. REPORT DATE
January, 1978
6. PERFORMING ORGANIZATION CODE
8. PERFORMING ORGANIZATION REPORT NO.
10. PROGRAM ELEMENT NO.
11. CONTRACT/GRANT NO.
68-02-2608
13. TYPE OF REPORT AND PERIOD COVERED
Final
14. SPONSORING AGENCY CODE
15. SUPPLEMENTARY NOTES 	 ~~ 	 —
The _ report is an .analysis of the energy required by various methods of reducing
sulfur dioxide emissions from coal-fired boilers. The energy required for limestone,
lime double alkali, magnesium slurry and Wellman-Lord/Alied flue gas scrubbing
systems is presented. The variation of energy requirements with coal sulfur content,
emission level achieved and plant size is presented. The energy required to
transport low sulfur coal to the mid-west or to physically clean sulfur from the
coal is presented also.
|17. KEY WORDS AND DOCUMENT ANALYSIS
[a. DESCRIPTORS

18. DISTRIBUTION STATEMENT
Release Unlimited
b. IDENTIFIERS/OPEN ENDED TERMS

19. SECURITY CLASS (This Report)'
Unclassified
20. SECURITY CLASS (This page)
Unclassified
c. COSATI Field/Group

21. NO. OF PAGES
124
22. PRICE

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