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FACILITY C C C K
CONTROL DEVICE VS VS VS ES
VS - VENTURI SCRUBBER ES -- CENTRIFIELD
SCRUBBER
Figure C-2. Particulate emissions from phosphate rock calciners
C-3
-------
BH -- baghouse
Figure C-3. Particulate emissions from phosphate rock grinders
0.020
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C-4
-------
DESCRIPTION OF FACILITIES
A. Oil-.fired (No. 6 fuel oil) rotary dryer designed to reduce the
moisture in phosphate rock from between 10 and 15 percent to less than
3 percent. Its production rate varies from 220 TPH to 440 TPH, depending on
the moisture content and the type of rock being processed. Florida land
pebble was dried during each of the EPA tests and during the first test
conducted by the operator. Flotation cell concentrates were being dried during
the second operator test. Emissions from the dryer are cleaned by a Ducon
venturi scrubber which has a pressure drop of 18 inches of water and uses
950 gal/min of recirculated water. EPA tests were conducted only while the
process was operating normally. EPA and operator particulate measurements
were performed using EPA Method 5, Visible emission measurements were made
by EPA at the scrubber exhaust in accordance with EPA Method 9.
B. One oil-fired rotary dryer and one oil-fired fluid bed dryer operated
1n parallel. Nominal production rates are 330 TPH for the rotary dryer and
165 TPH for the fluid bed dryer; however, actual production rate is dependent
on the amount of moisture and type of rock fed to the dryers. Both dryers
were operated normally at full capacity and processed 100 percent Florida
land pebble for each of the EPA tests. Emissions from both dryers are
partially cleaned by two parallel Impingement scrubbers (one for each dryer).
Emissions from the scrubbers are combined and ducted to a two-stage wet
electrostatic precipitator (ESP) which has a total collecting area of
50,600 square feet and a gas velocity of 1.53 feet per second. The cleaned
gas exits the ESP from two vertical stacks. The ESP was reportedly designed
for approximately twice the volume of .gas currently being processed. EPA
C-5
-------
particulate measurements were performed using EPA Method 5. The operator
conducted measurements using the State of Florida Department of Pollution
Control Method. Visible emission observations were made at the ESP
exhausts in accordance with EPA Method 9.
C. Fluid bed, oil-fired (No. 2 fuel oil) calciner used to remove
moisture and organics from phosphate rock. Designed to calcine 70 TPH,
but the operator has increased the calcining capacity to 8'0 TPH by drying a
portion of the feed prior to calcination. Calciner emissions are cleaned
by an ARCO venturi scrubber Y(hich has a pressure drop of 12 inches of
water and uses about 600 gal /mi n recirculated water. Tests were conducted
only while the process was operating normally. EPA and company particulate
measurements were performed using EPA Method 5. The results of the tests by the
Company are reported in Tables C-6 and C-7. Fluoride tests were performed
'EPA Method 13, and visible emissions were recorded using EPA Method 9.
D. Kennedy Van Saun ball mill used to grind phosphate rock. Production
throughput is nominally rated at 124 TPH, but is dependent on the degree of
fineness to which the rock is ground. Emissions from the grinder are cleaned
by a Mikro-Pulsaire baghouse. Tests were conducted only during normal
process operation, Particulate measurements were performed using EPA Method
5. Visible emissions were not recorded.
E, Raymond roller mill used to grind dried phosphate rock. Production
throughput is nominally rated at 35 TPH, but is dependent on the degree of
C-6
-------
fineness to which the rock is ground. During the first two tests, rock
was ground to 65 percent through 200 mesh, and it was ground to 90 percent
through TOO mesh (65 to 85 percent through 200 reesh), during the third test.
Emissions from the grinder are cleaned by a baghouse. Tests were conducted only
during, periods when the process was operatina normally. Particulate measurements
were performed using EPA Method 5. Visible emission observations were made at
the baghouse exhaust.
F. One roller mill and one ball mill operated in parallel. Production
rates cannot be measured accurately, but experience shows that the roller rail!
normally operates, at 27.5 TPH and ball mill at 50 TPH. The method used
to determine if mills are operating at full capacity is by the amperage
reading of the mill motors and fans. Mills were operated at full capacity during
all EPA tests. Emissions from both grinders are combined and cleaned by a
baghouse which has an air-to-cloth ratio of 4. to 1. Tests were conducted
only while the process was operating normally. EPA particulate measurements
were performed using EPA Method 5. Particulate measurements made by the
operator were performed using Western Precipitation Method WP-50. The results
are presented 1n Table C-12. Visible emission observations were made at the
baghouse exhaust in accordance with EPA Method 9.
G. Harding ball mill used to grind calcined phosphate rock to 50 percent
minus 200 mesh. Production throughput is nominally rated at 60 TPH.
Emissions from the grinder are cleaned by a Mikropul, pulse-air cleaned bag-
house with an air-to-cloth ratio of about 5 tol. Tests were conducted only
C-7
-------
during periods when the process was operating normally. EPA and company
participate measurements were performed using EPA Method 5. Results of the
Company tests are shown in Table C-14. Visible emission observations were made
at the baghouse exhaust in accordance with EPA Method 9.
H. Pneumatic system for transferring ground phosphate rock from a storage
silo at a phosphate rock grinder to a storage silo at a wet-process phosphoric
acid plant. About 60 percent of the rock transferred is small enough to
pass through a 200 mesh screen. The system was transferring about 60 tons of
ground rock per hour, which is its normal operating rate. It has an exhaust
gas flow rate of about 1700 dscfm. Emissions from the system pass first
through a cyclone and then through a Mikro-Pulsaire baghouse which has an
air-to-cloth ratio of about 4 to 1. Visible emission measurements were
made at the baghouse exhaust in accordance with EPA Method 9.
I. Pneumatic system for transferring ground phosphate rock from a
storage silo at a phosphate rock grinder to a storage silo at a wet-process
phosphoric acid plant. About 60 percent of the rock transferred is small
enough to pass through a 200 mesh screen. The system is designed to transfer
about 47.5 tons of ground rock per hour,'but can transfer a maximum of
87.5 tons per hour. It was operating at about 77.5 tons per hour during the
EPA tests. Emissions from the transfer system exhaust through a cyclone to
a Mikro-Pulsaire baghouse which has 36 bags, each of which are 96 inches
long by 4.5 inches in diameter. The exhaust gas flow rate is about 2,500
dscfm and" the air-to-cloth ratio is about 8 to.!.' Visible emission measurements
C-8
-------
were made at the baghouse exhaust in accordance with EPA Method 9.
0. Pneumatic system for transferring ground phosphate rock from
a phosphate rock grinder to a storage silo at a run-of-pile triple super-
phosphate plant. About 70 percent of the rock transferred is small enough
to pass through a 200 mesh screen. The system was transferring about
15 tons of ground rock per hour, which is its normal operating rate.
It has an exhaust gas flow rate of about 2000 dscfm. Emissions from the
system pass through a cyclone to a baghouse which has 25 bags, each of
which are 96 inches long by 4.5 inches in diameter, yielding an air-tordoth
ratio of about 9 to 1. Visible emission measurements were made at the
baghouse exhaust in accordance with EPA Method 9.
K. Fluid, bed, natural gas-fired calciner used to remove moisture
and organics from phosphate rock. Designed to calcine 46 tph, but
operator has difficulty maintaining the design.product!on rate because
of lack of surge capacity between calciner and grinder. Calciner emissions
are cleaned by an Entoleter Centrifield scrubber which operates in
a range of 20 to 30 inches of water pressure drop. Parti oil ate measure-
ments were conducted by the operator using EPA Method 5 while the
calciner was operating normally. Visible emissions were recorded by EPA
using EPA Method 9. Visible emission measurements were not recorded
simultaneously with the Method 5 tests.
C-9
-------
TABLE C-l
FACILITY A
Summary of Results of Tests of a Dryer
Run Number
Date-
Test Time - Minutes
Production Rate - TPH
Stack Effluent (From a Scrubber)
Flow rate - ACFM
Flow rate - DSCFM
Temperature - °F
Water vapor - Vol . %
Visible Emissions at
Collector Discharge -
% Qoacity
Parti oil ate Emissions
Probe and filter catch
gr/DSCF
gr/ACF
Tb/hr
Ib/ton
Total catch
gr/ACF
Ib/hr
Ib/ton
1
3/18/75
108
250
6,786
3,289
153
27.4
0.014
0.009
9.07
0.036
0.058
0.037
36.57
0.146
2
3/18/75
108
235
115,967
74,553
152
25.7
See Tables
0.017
0.011
11.14
0.047
0.042
0.028
27.46
0.117
3
3/19/75
108
240
116,437
73,782
153
26.6
C-l 5 through
0.013
0.008
8.04
0.034
0.051
0.032
32.44
0.135
Averac
-
108
242
116,397
73,875
153
26.6
C-17
0.015
0.009
9.42
0.039
0.051
0.032
32.16
0.133
C-10
-------
TABLE c-2
FACILITY A
Summary of Results of Tests of a Dryer
Run Number
Date
Test Time - Minutes
Production Rate - TPH
Stack Effluent (From a Scrubber)
Flow rate - ACFM
Flow rate - DSCFM
Temperature - °F
Water vapor - Vol. %
Visible Emissions at
Collector Discharge -
% Ooacity
Particulate Emissions
1
9/4/74
9/8/74
Average
360
109,000
65,000
160
24.8
Probe and filter catch
gr/DSCF a
gr/ACF a
Tb/hr
Ib/ton
Total catch
gp/DSCFa
gr/ACF a
Ib/hr
Ib/ton
' Calculated
NR - Not Reported
0.025
0.015
14.7
0.041
0.046
0.027
26.7
0.074
0.018
0.011
10.0
0.036
0.040
0.024
21.5
0.060
0.022
0.013
12.3
0.038
0.043
0.026
24.1
0.067
-------
TABLE C-3
FACILITY B
Summary of Results of Tests of a Dryer
Run Number
Date
Test Time - Minutes
Production Rate - TPH
Stack Effluent (From an ESP)
Flow rate - ACFM
Flow rate - DSCFM
Temperature - °F
Water vapor - Vol. %
Visible Emissions at
Collector Discharge -
% Ooacity
Particulate Emissions
Probe and filter catch
gr/DSCF
gr/ACF
Tb/hr
Ib/ton
Total catch
gr/DSCF
gr/ACF
Ib'/hr
Ib/ton
1
3/20/75
108
394
134,463
113,144
112
9.2
0.012
0.010
11.91
0.030
0.015
0.013
14.66
0.037
2
3/20/75
108
394
133,566
110,758
115
10.0
See Tables
0.013
0.010
12.08
0.031
0.016
0.014
15.06
0.038
3
3/24/75
108
379
129,084
111,918
104
7.46
C-18 through
0.005
0.005
5.23
0.014
0.009
0.008
8.80
0.023
Avera<
-
108
389
132,371
111,940
no
8.9
C-20
0.010
0.008
9.74
0.025
0.013
o.on
12.84
0.033
c-i*
-------
TABLE C-4"
FACILITY B
Summary of Results of
Tests of a Dryer
Date
Test Time - Minutes
Production Rate - TPH
Stack Effluent (From an ESP)
Flow rate - ACFM
Flow rate - DSCFM b
Temperature - °F
Water vapor - Vol. %
Visible Emissions at
Collector Discharge -
% Ooacity
Particulate Emissions
Probe and filter catch
gr/DSCF
gr/ACF
Tb/hr
Ib/ton
Total'catch
gp/DSCF C
gr/ACF c
Ib/hr
lb/tonc
6/10/74 - 8/14/74
NR
423
124,373
115,348
NR
NR
NR
NR"
NR
NR
NR
0,023
0.021
22.8
0.054
'aAverage of 11 tests, 9 of which were performed while both dryers were fired with
natural gas.
Calculated; assuming a stack gas temperature of 110°F.
Calculated.
NR - Not Reported
C-T?
-------
Run Number
Date
TABLE C-5
FACILITY c
Summary of Results
of Tests of a Caldner
1 2,3 4 5 6
4/8/75 4/8/75 4/9/75 4/9/75 4/10/75 4/10/75
Average
Test Time - Minutes
Production Rate - TPH
Stack Effluent (From a
Flow rate - ACFM
Flow rate - DSCFM
Temperature - °F
Water vapor - Vol.
Visible Emissions at
Collector Discharge -
% Opacity
Parti cul ate Emissions
120
80
Scrubber)
47,197
25,319
141.5
% ' 25.1
0
120
, 80
50,160
27,764
143.5
22.6
0
120
80
51 ,456
28,407
145.8
22.5
0
120
80
54,719
28,005
158.5
26.7
0
120
80
50,324
27,525
146.0
23.1
0
120
80
49,262
26,338
144.6
25.0
0
120
80
'50,520
27,226
146.7
24.2
0
Probe and filter catch
gr/DSCF
gr/ACF
Ib/hr
Ib/ton
Total catch
gr/DSCF
gr/ACF
Ib/hr
Ib/ton
NR - Not Recorded
0.038
0.020
8.18
0.10
0.040
0.021
8.62
0.11
0.055
0.030
13.10
0.16
0.057
0.031
13.46
0.17
0.048
0.027
11.8
0.15
0.051
0.028
12.49
0.16
0.046
0.023
10.98
0.14
0.057
6.029
13.68
0.17
0.041
0.023
9.75
0.12
0.044
0.024
10.44
0.13
0.053
0.028
11.99
0.15
0.067
0.035
15.03
0.19
0.047
0.025
9.20
0.14
0.053
0.028
12.29
0.15
C-14
-------
TABLE C-6
FACILITY C
Summary of Results
of Tests of a Calciner
Run Number
Date
Test Time - Minutes
Production Rate - TPH
Stack Effluent (From a Scrubber)
Flow rate - ACFM
Flow rate - DSCFM
Temperature - °F
Water vapor - Vol. %
Visible Emissions at
Collector Discharge -
% Ooacity
Particulate Emissions
Probe and filter catch
gr/DSCF
gr/ACF
Tb/hr -
Ib/ton
Total catch
gp/DSCF
gr/ACF
Ib/hr
Ib/ton
1
10/2/73
10/3/73
10/3/73
Average
98
51.7
46,850
29,558
131
12.38
NR
0.034
0.021
8.54
0.17
NR
NR
NR
NR
98
35.9
38,391
25,540
124
9.51
NR
0.043
0.028
9.32
0.23
NR
NR '
NR
NR
98
35.9
41 ,069
26,885
126
10.81
NR
0.049
0.032
11.30
0.31
NR
NR
NR
NR
98
41.2
42,103
27,328
127
10.90
-
0.042
0.027
9.46
0.24
-
-
-
«•
NR - Not Reported
C-15
-------
Run Number
Date
Test Time - Minutes
Production Rate - TPH
Stack Effluent (From a Scrubber)
Flow rate - ACFM
Flow rate - DSCFM
Temperature - °F
Water vapor - Vol. %
Visible Emissions at
Collector Discharge -
% Ooacity
Parti oil ate Emissions
TABLE C-7
FACILITY C
Summary of Results
of Tests of a Calciner
1 2
Average
120 •
64.8
48,451
32,756
132
6.37
Probe and filter catch
gr/DSCF
gr/ACF
Tfa/hr
Ib/ton
Total catch
gr/DSCF
gr/ACF
Ib'/hr
Ib/ton
0.043
0.029
12.03
0.186
NR
NR
NR
NR
0.020
0.013
5.58
0.086
NR
NR
NR
NR
0.032
0.021
8.80
0.136
-
•
-
..
a Two of three tests were averaged. The third test was invalidated by sample contamination.
NR - Not Reported . . • ,
C-16
-------
TABLE C-7a
FACILITY K
Summary of Results
Of Tests of a Calciner
Run Number
Date
Test Time - Minutes
Production Rate - TPH
Stack Effluent
Flow rate - ACFM
Flow rate - DSCFM
Temperature - °F
Water vapor - Vol. %
Visible Emission at
Collector Discharge - % Opacity
Particulate Emi ssions
Probe and filter catch
1
3/9/75
NR
27
2
9/2/75
NR
25
3
12/17/75
NR
25
11
NR
,100 "
NR
NR
NR
NR
10,900
NR
NR
NR
NR
10,900
NR
NR
NR
Average
25.7
10,967
gr/DSCF
gr/ACF
Ib/hr
lb/ton
Total catch
gr/DSCF
gr/ACF
Ib/hr
Ib/ton
UT
0.023
NR
2.21
0.082
0.025
NR
2.37
0.095
0..028
NR
2.67
0..107
0.025
7.26
0.094
NR
NR
NR
NR
NR
NR
NR
NR
NR
NR
NR
- NR
(1)
Calculated from information submitted by operator
NR - Not Reported
C-16a
-------
-------
Run Number
Date
TABLE C-8
FACILITY C
Summary of Results
of Tests of a Calciner
2 3 4
Average
4/4/75 4/5/75 4/8/75 4/8/75 4/9/75 4/10/75
120
80
120
80
120
80
120
80
120
80
120
80
Test Time - Minutes 120
Production Rate - TPH 80
Stack Effluent (From a Scrubber)
Flow rate - ACFM 53,213 50,116 47,101 49,251 55,430 49,563 50,779
27,965 27,752 26,267 26,803 28,275 26,663 27,288
145.0 143.3 144.4 152.5
22.3 21.9 23.8 27.6
Flow rate - DSCFM
Temperature - °F 146.3
Water vapor - Vol. % 26.1
143.5
24.6
145.8
24.5
Visible Emissions at
Collector Discharge -
% Opacity
Fluoride Emissions
Total catch
gr/DSCF
gr/ACF
Ib/hr
Ib/ton
0.00020 0.00038 0.00092 0.00046
0.00010 0.00021 0.00051 0.00025
0.05 0.09 0.21 0.11
0.0006 0.0011 0.0026 0.0014
0.00035 0.00104
0.00018 0.00056
0.08 0.24
0.0010 0.0030
0.00056
0.00030
0.13
0.0016
C-17
-------
Run Number
TABLE C-9
FACILITY D
Summary of Results
of Tests of a Grinder
1 '2
Average
Date
Test Time - Minutes
•>
Production Rate - TPH
Stack Effluent (From a Baghouse)
Flow rate - ACFM
Flow rate - DSCFM
Temperature - °F
Water vapor - Vol . %
Visible Emissions at
Collector Discharge -
% Ooacity
Parti cul ate Emissions
Probe and filter catch
gr/DSCF
gr/ACF
Tb/hr
"Ib/ton
Total catch
giVDSCF
gr/ACF
Ib/hr
Ib/ton
1/11/73
128
121
15,200
13,200
115
5.80
NR
0.0102
0.0089
1,154
0.0095
0.0132
0.0114
1.49
0.0123
1/11/73
128
131
14,700
12,800
115
6.10
NR
0.0115
0.0100
1.270
0.0097
0.0155
0.0134
1.70
0.0130
1/12/73
128
120 '
14,900
13,000
118
5.30
NR
0.0078
0.0068
0.869
0.0072
0.0100
0.0087
1.11
0.0093
-
128
124
14,900
13,600
116
5.70
NR
0.0098
0.0072
1.098
0.0088
0.0129
0.0095
1.43
• 0.0012
NR - Not Recorded
C-18
-------
Run Number
Date
TABLE C-10
• FACILITY E
Summary of Results
of Tests of a Grinder
Test Time - Minutes
Production Rate - TPH
Stack Effluent (From a Baghouse)
Flow rate - ACFM
Flow rate - DSCFM
Temperature - °F
Water vapor - Vol. %
Visible Emissions at
Collector Discharge -
% Ooacity
Particulate Emissions
Probe and filter
1
2/16/73
120
36.0
3,295
2,720
161
5.32
2
2/16/73
120
36.0
3,256
2,654
161
6.05
3
2/16/73
120
33.0
3,386
2,751
161
6.53
Average
-
120
35.0
3,312
2,708
161
5.97
NR
NR
NR
NR
gr/DSCF
gr/ACF
Tb/hr
Ib/ton
Total ' catch
.WDSCF
gr/ACF
Ib/hr
Ib/ton
i 1
0.0085
0.0070
0.198
0.0055
0.0149
0.0122
0.347
0.0096
0.0066
0.0054
, 0.149
0.0041
0.0178
0.0146
0.406
0.0113
0.0044
0.0035
0.102
0.0031
0.0080
0.0065
0.188
0.0057
0.0065
0.0053
0.150
0.0042
0.0136
o.om
0.314
0.0089
NR - Not Reported
c-iy
-------
TABLE C-ll
FACILITY F
Summary of Results
of Tests of a Grinder
Run Number
Date
Test Time - Minutes
Production Rate - TPHa
Stack Effluent (From a Baghouse)
Flow rate - ACFM
Flow rate - DSCFM
Temperature - °F
Water vapor - Vol. %
Visible Emissions at
Collector Discharge -
% Ooacity
Parti oil ate Emissions
1
3/25/75
120
77.5
8,385
6,676
146
9.47
2
3/25/75
120
77.5
8,582
6,809
155
8.47
3
3/26/75
120
77.5
7,897
6,449
139
8.79
Average
-
120
77.5
8,288
6,645
147
8.91
Probe and filter catch
gr/DSCF
gr/ACF
Tb/hr
Ib/ton
Total ' catch
gp/DSCF
gr/ACF
Ib/hr
m/4-nn
0.002
0.002
0.117
0.0015
0.003
0.002
0.159
0.0021
0.002
0.001
0.099
0.0013
0.003
0.002
0.159
0.0021
0.002
0.001
0.093
0.0012
0.002
0.002
0.116
0.0015
0.002
0.001
0.103
0.0013
0.003
0.002
0.145
0.0019
the normal production rate when
in U. was calc.Uted
using the normal production rate
C-20
-------
Run Number
Date
TABLE C-12
. FACILITY F
Summary of Results
of Tests of a Grinder
Average9
V3/74 - 6/27/74
Test Time - Minutes
Production Rate - TPH
Sta;ck Effluent (From.a Baghouse)
Flow rate - ACFM
Flow rate - DSCFM
Temperature - °F
Water vapor - Vol. %
Visible Emissions at
Collector Discharge -
% Ooacity
Parti oil ate Emissions
Probe and filter catch
gr/DSCF
gr/ACF
Tb/hr
]b/ton ,
Total'catch
gi»/DSCFb
gr/ACF
Ib/hr
Ib/ton
a Average of 15 tests.
Calculated.
NR - Not Reported
NR
NR
NR
5,133
NR
NR
NR
NR
NR
NR
NR
0.0028
NR
0.12
NR
-------
TABLE C-13
FACILITY G
Summary of Results
of Tests of a Grinder
Run Number
Date
Test Time - Minutes
Production Rate - TPH
Stack Effluent (From a Baghouse)
Flow rate - ACFM
Flow rate - DSCFM
Temperature - °F
Water vapor - Vol. %
Visible Emissions at
Collector Discharge -
% Qoacity
Particulate Emissions
1
4/5/75
200
81.4
6,713
4,194
233
0.0
2
4/7/75
200
81.0
6,830
4,286
231
0.0
3
4/7/75
200
80.8
6,446
3,983
241
0.0
Averagi
-
200
81.1
6,663
4,124
235
0.0
0-
Probe and filter catch
gr/DSCF
gr/ACF
Tb/hr
Ib/ton
Total catch
giVDSCF
gr/ACF
Ib/hr
Ib/ton
•
0.0014
0.0009
0.05
0.0006
0.0015
0.0009
0.05
0.0006
0.0034
0.0021
0.12
0.0015
0.0038
0.0024
0.14
0.0017
0.0016
0.0011
0.06
0.0007
0.0039
0.0024
0.13
0.0016
0.0021
0.0014
0.08
0.0009
0.0031
0.0019
0.12
0.0013
C-22
-------
TABLE C-14
FACILITY G
Summary of Results
of Tests of a Grinder
Run Number
Date
Test Time - Minutes
Production Rate - TPH
Stack Effluent (From a Baghouse)
Flow rate - ACFM
Flow rate - DSCFM
Temperature - °F
Water vapor - Vol. %
Visible Emissions at
Collector Discharge -
% Ooacity
Particulate Emissions
1
10/3/73
120
52
8,242
5,635
159
0.84
2
10/3/73
120
52
8,423
5,661
177
0.00
3
10/3/73
120
52
8,058
5,408
177
0.00
Averac
-
120
52
8,241
5,568
171
0.28
NR
NR
NR
Probe and filter catr.h
gr/DSCF
gr/ACF
•Tb/hr
Ib/ton
Total ' catch
gr/DSCF
gr/ACF
Ib/hr
Ib/ton
0.0047
0.0032
0.23
0.0044
NR
NR
NR
NR
0.0061
0.0041
0.30
0.0057
NR
NR
NR
NR
0.0038
0.0025
0.18
0.0034
NR
NR
NR
NR
0.0049
0.0033
0.24
0.0045
*•
—
NR - Not Reported
C-23
-------
Table C-lb
FACILITY A
SUMMARY OF VISIBLE EMISSIONS
Date: March 18, 1975
Type of Plant: Phosphate Rock Dryer
Type of Discharge: Stack from scrubber
Location of Discharge: Top of stack
Height of Point of Discharge: 96 feet
Description of Background: Gray sky
Description of Sky: Overcast
Hind Direction: East
Color of Plume:- White
Interference of Steam Plume: Yes •
Duration of Observation: 3 nours, 9 minutes
SUMMARY OF AVERAGE OPACITY
Distance from Observer to Discharge Point:
2000 feet
Height of Observation Point: Ground level
Direction of Observer from Discharge Point:
Nortnwest
Wind Velocity:
Detached Plume:
No
SUMMARY OF AVERAGE OPACITY
Time
Set Number Start End
1 9:00 9;06
2 *
3
4
5
6
7
8
9
10
11
12
13
14
15
16
17
13
19
20
Opaci ty
Average
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
Time
Set Number Start End
21
22
23
24
25
26
27
28
29
30
31
32
33
34
35
36
37
38
39
40
Opaci ty
Average
0
0
0
0
0 .
u
0
0
0
0
Subsequent sets were each of 6-minutes duration, and there were no time lapses between
sets.
C-24
-------
Tablo C-15, continued.
SKETCH SHOWING HOW OPACITY VARIED WITH TIME-
g 10
a.
O
s
0
234
TIME, hours
C-25
-------
Table C-16
FACILITY A
SUMMARY OF VISIBLE EMISSIONS
Date: March 18, 1975
Type of Plant: Phosphate roc* dryer
Type of Discharge: Stack from scrubber
Location of Discharge: Top of stack
Height of Point of Discharge: 96 feet
Description of Background: Cloudy sky
Description of Sky: Cloudy
Wind Direction: South-West
Color of Plume: White
Interference of Steam Plume: Yes
Duration of Observation: 2 hours, 2£ minutes
SUMMARY OF AVEPvAGE OPACITY
Distance from Observer to Uisciiarge Point:
luuu
Height of Observation Point: Ground level
Direction of Observer from Jiscnarge Point:
ilorth-'.fest
Wind Velocity:
Detached Plume:
mi/rir
No
SUMMARY OF AVERAGE OPACITY
Ti nie
Set dumber Start End
1 4:22 4:28
2 *
3
4
5
6
7
8
9
10
11
12
13
14
15
16
17
18
19
20
Opacity
Average
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
Time Opacity
Set Number Start End Average
21 0
22 0
23 u
24 . • 0
2s • 0
* Subsequent sets were each of 6-minute durations, and there were no time lapses
between sets.
C-26
-------
Table C-16, continued.
SKETCH SHOWING HOW OPACITY VARIED WITH TIME:
15
10
o.
s-"
2 3
TIME, hours
C-27
-------
Table C-17
FACILITY A
SUMMARY OF VISIBLE EMISSIONS
Date: March 19, 1975
Type of Plant: Phosphate rock dryer
Type of Discharge: Stack from scrubber
Location of Discharge: Top of stack
Height of Point of Discharge: 96 feet
Description of Background: Blue sky
Description of Sky: Clear
Wind Direction: Vlest Northwest
Color of Plume: White
Interference of Steam Plume: Yes
Duration of Observation: 2 hours, 51 minutes
SUMMARY OF AVERAGE OPACITY
Distance from Observer to Discharge Point:
100 feet
Height of Observation Point: Ground level
Direction of Observer from Discharge Point:
Soutn
Wind Velocity: 15-30
Detached Plume: No
SUMMARY OF AVERAGE OPACITY
Set Number
1
2
3
4
5
6
7
8
9
10
11
12
13
14
15
16
. 17
18
19
20
Time Opacity
Start End Averaqe
11:30 11:36 0
* ' 0
0
0
0
0
0
0
0
0
0
0
0
0
0
• o
0
0
0
0
Time
Set Number Start End
21
22
23
24
25
26
27
28
"
Opaci ty
Averaqe
0
0
0
0
0
0
0
0
* Subsequent sets were each of 6-minutes duration, and there:were no time lapses
between sets.
C-28
-------
Tibia C-17, continued.
SKETCH SHOWING HOW OPACITY VARIED WITH TIME:
15
V
&
2 3
TIME, hours
C-29
-------
Table C-18
FACILITY B
SUMMARY OF VISIBLE EMISSIONS *
Date: March 20, 1975
Type of Plant: Phosphate rock dryer
Type of Discharge: Stack from electrostatic
Location of Discharge: Stac* precipitat
Height of Point of Discharge: >£#90 feet
Description of Background: Blue sky
Description of Sky: Clear
Wind Direction: West
Color of Plume: White
Interference of Steam Plume: Yes
Duration of Observation: 2 hours, 15 minutes
SUKMARYOF AVERAGE OPACITY
Distance from Observer to Discharge Point:
feet
Height of Observation Point: Ground level
Direction of Observer from Discharge Point:
South Soutueast
Wind Velocity: 8
Detached Plume:
Set Number
1
2
3
4
5
6
7
8
9
10
11
12
13
14
15
16
17
18
19
20
Time Opacity
Start End Averaqe •
2:00 2:06 5.0
** 7.7
6.7
5.0
5.8
6.7
7.1
5.0
5.4 .
5.6
5.6
5.0
5.0
4.6
5.0
5.0
' 5.0
5.0
4.6
5.0
Time
Set Number* Start End
21
22
23
24
25
26
27
28
29
30
31
32
33
34
' 35
36
37
38
39
40
Opacity
Average
5.0
6.9
*Four observers made simultaneous readings (two observers for each of two stacks). The
greatest of their readings is reported.
**Subsequent sets were each of 6-minutes duration, and there were no time lapses
between sets.
C-3U
-------
Table C-18, continued.
SKETCH SHOWING HOW OPACITY VARIED WITH TIME:
3
15
«
5
.
DIM
2 34
TIME, hours
C-31
-------
Table c-19
FACILITY B
SUMMARY OF VISIBLE EMISSIONS*
Date: March 20, 1975
Type of Plant: Phosphate rock dryer
Type of Discharge: Stack from electrostatic
Location of Discharge: Top of stacRreclp
Height of Point of Discharge:^9° feet
Description of Background: Clear blue sky
Description of Sky: Clear
Wind Direction: Northeast
Color of Plume: White
Interference of Steam Plume: Yes
Duration of Observation: 2 hours
Distance from Observer to Discharge Point:
150 feet
Height of Observation Point: Ground level
Direction of Observer from Discharge Point:
South Southeast
Wind Velocity: 10
Detached Plume: Yes
SUMMARY
Set Number
1
2
3
4
5
6
7
8
9
10
Tl
12
13
14
15
16
17
18
19
20
OF AVERAGE OPACITY
Time Opacity
Start End Average
5:17 5:23 3.8
** ' ' 4.6
2.3
2.9
1.0
3.1
1.7
0.8
0.6
0.8
0.4 '
2.1
2.9
1.2
0
0
0
0
0
0
SUMMARY OF AVERAGE
Time
Set Number Start End
21
22
23
24
25
26 '
27
28
29
30
31
32
33
34
35
36
37
38
39
. 40
OPACITY
Opacity
Average
0
0
*Four observers made simultaneous readings (two observers for each ;of two stacks). Trie
greatest of their readings is reported.
**Subsequent sets were each of 6-minutes duration, and there were no time lapses between
sets.
Cr32
-------
Table C-H9, continued.
SKETCH SHOWING HOW OPACITY VARIED WITH TIME:
15
| 10
S
a
> 5
niiiiiiiiiiiiiiii
2 3
TIME, hours
C-33
-------
Table C-20
FACILITY B
SUMMARY OF VISIBLE EMISSIONS *
Date: March 24, 1975
Typ& of Plant: Phosphate rock dryer
Type of Discharge: Stack from electrostatic
3 preci pita tor
• Location of Discharge: Stack
Height of Point of Discharge: 90 feet
Description of Background: Cloudy sky
Description of Sky:- Partly cloudy
Wind Direction: Southwest
Color of Plume: White
•Interference of Steam Plume: Yes
Duration of Observation: 103 minutes, 15 seconds
Distance from Observer to Discharge Point:
. 120 feet
Height of Observation Point: Ground level
Direction of Observer from Discharge Point:
Southeast
Wind Velocity:
Detached Plume:
No
5UMWU
Set Number
- 1
2
3
4
5
6
7
8
9
10
11
12
13
14
15
16
17
18
19
20
Of OF AVERAGE OPACITY
Time Opacity
Start End Averaqe
1:05 1:11 4.8
** ' 4.8
4.0
4.5
4.4
4.7
5.2
4.8
4.6
4.8
2.9
4.0
3.8
3.9
4.0
4.2
0
4.0
SUMMARY OF AVERAGE
Time
Set Number Start End
21
22
23
24
25
26
27
28
29
30
31
32
33
34
35
36
37
38
39
40
OPACITY
Opacity
Averaqe
*•
*Four observers made simultaneous readings (two observers for each of two stacks). The
greatest of their readings is reported.
**Subsequent sets were each of 6-minutes duration, and there were no time lapses between
sets.
C-34
-------
Table C-20, contimMd.
15
| 10
I
> 5
o
i 0
jii
SKETCH SHOWING HOW OPACITY VARIED WITH TIME:
2 3
TIME, hours
C-35
-------
Table C-21
FACILITY C
SUMMARY OF VISIBLE EMISSIONS*
Date: APr1l 4, 1975
Type of Plant: Phosohate rock calciner
Type of Discharge: participate
Location of Discharge: Stack *rom scrubber
Height of Point of Discharge: 105 feet
Description of Background: Sky
Description of Sky: Overcast
Hind Direction: North
Color of Plume: white
Interference of Steam Plume: Yes
Duration of Observation: 2 hours, 5 minutes
Distance from Observer to Discharge Point:
. 1440 feet
Height of Observation Point:Ground level
Direction of Observer from Discharge Point:
South Southeast
Wind Velocity: 3-10
Detached Plume: No
SUMMA1
Set Number
1
2
3
4
5
6
7
8
9
10
n
12
13
14
15
16
17
18
19
20
*Y OF AVERAGE OPACITY
Time Opacity
Start End Averaqe
2:50 2:56 0
** 0
0
' ' 0
0
0
0
• o
0
0
0
0
0
0
0
0
0
0
0
0
' SUMMARY OF AVERAGE OPACITY
• Time Opaci ty
Set Number Start End Average
-21
22 .
23
24
25
26
27
28
29
30
31
32
33
34
'35
36
37
38 -
39
40
*Two observers made simultaneous readings. The greater of their readings is reported.
**Subsequent sets were each of 6rm1nutes duration, and there were no time lapses between
sets. . .
-------
Tattle C-21, continued.
SKETCH SHOWING HOW OPACITY VARIED WITH TIME:
15
10
5
2 3
TIME, hours
C-37
-------
Table C-22
FACILITY C
SUMMARY OF VISIBLE EMISSIONS *
Date: April 5, 1975
Type of Plant: Phosphate rock calciner
Type of Discharge: Participate
Location of Discharge: Stack from scrubber
Height of Point of Discharge: 105 feet
Description of Background: Sky
Description of Sky: Overcast
•Hind Direction: South
Color of Plume: White
Interference of Steam Plume: Yes
Duration of Observation: 2 hours, 5 minutes
SUMMARY OF AVERAGE OPACITY
Distance from Observer to Discharge Point:
600 feet
Height of Observation Point:Ground leve1
Direction of Observer from Discharge Point:
East
Wind Velocity: 15-2b
Detached Plume: No
SUMMARY OF AVERAGE OPACITY
Time
Set Number Start End
1 8:45 9:01
2 **
3
4
5
6
7
3
9
10
11
12
13
14
15
16
17
18
19
20
Opaci ty
Averaqe
0
0
0
0 .
0
0
0
0
0
0
o •
0
0
0
0
0
0
0
0
0
Time Opacity
Set Number Start End ' Average
21
22
23
24
25
26
27
28
29
30
31
32
33
34
35
36
37 '
38
39
40
*Two observers made simultaneous readings. The greater of their readings is reported.
**Subsequent sets were each of 6-minutes duration, and there were no time lapses between
sets.
C-38
-------
Table C-22, continued.
SKETCH SHOWING HOW OPACITY VARIED WITH TIME:
s
o>
a.
«3
15
10
Z 3
TIME, hours
C-39
-------
Table C-23
FACILITY C
SUMMARY OF VISIBLE EMISSIONS *
Date:April 9, 1975
Type of Plant:" Phosphate rock calciner
Type of Discharge: Participate
Location of Discharge: Stack from scrubber
Height of Point of Discharge: 105 feet
Description of Background: Snowy sky
Description of Sky: Overcast
Wind Direction: South
to!or of Plume: White
Interference of Steam Plume: Yes
Duration of Observation: 1 hour, 45 seconds
SUMMARY OF AVERAGE OPACITY
Distance from Observer to Discharge Point:
1/4 mile
Height of Observation Point: Ground le.val
Direction of Observer from Discharge Point:
Southeast
Wind Velocity: 5-20
Detached Plume: I>)0
SUMMARY OF AVERAGE OPACITY
Set Number
1
2
3
4
5
6
7 •
8
9
10
11
ia
13
14
15
16
17
18
19
20
Time Opacity
Start End Average
8:50 8:56 0
** • 0
0
0
0
0
0
0
0
0
Time
Set Number Start End
21
22
23 ,.
24
25
26
.27
28 '
29
30
31
32
33
34
35
36
37
38
39
40
Opaci ty
Average
*Two observers made simultaneous readings. The greater of their readings is reported.
**Subsequent sets were each of 6-minutes duration, and there were no time lapses between
sets.
C-40
-------
Table C-23, continued.
SKETCH SHOWING HOW OPACITY VARIED WITH TIME:
15
I 10
u
£
is
cj
2 3
TIME, hours
C-41
-------
Table C-24
FACILITY C
SUMMARY OF VISIBLE EMISSIONS *
Date: April 9, 1975
Type of Plant: Phosphate rock calciner
Type of Discharge: Particulate
. Location of Discharge: Stack from scrubber
Height of Point of Discharge: 105 feet
Description of Background: skV
Description of Sky: Overcast
•Hind Direction: South
Color of Plume: VJh1te
Interference of Steam Plume: Yes
Duration of Observation: 2 Hours, 0 minutes
Cf
Distance from Observer to Discharge Point:
1440 feet
Height of Observation Point: Ground level
Direction of Observer from Discharge Point:
Southeast
Wind Velocity: 2-3
Detached Plume: Ho
SUMMARY OF AVERAGE OPACITY
Set Number
1
2
3
d
t
5
6
7
*
8
9
10
11
1 l
12
13
14
15
16
17
18
19
I «*
20
Time Opacity
Start End Average
5:00 5:06 0
** • o
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
Time
Set Number Start End
21
22
23
24
25
26
27
28
29
30
31
32
33
34
35
36
37
38
39
40
Opacity
Averaqe
sets.
C-42
-------
Table C-24, continued.
SKETCH SHOWING HOW OPACITY VARIED WITH TIME-
5 10
0.
2 3
TIME, hours
C-43
-------
Table C-25
FACILITY C
SUMMARY OF VISIBLE EMISSIONS*
Date: April 10, 1975
Type of Plant: Phosphate Rock Calciner
Type of Discharge: Particulate
Location of Discharge: Stack from Scrubber
Height of Point of Discharge: los feet
Description of Background: Sky
Description of Sky: Overcast
Hind Direction: East
'Color of Plume: White
Interference of Steam Plume: Yes
Duration of Observation: 2 hours 0 min
SUMMARY OF AVERAGE OPACITY
Distance from Observer to Discharge Point:
1440 feet
Height of Observation Point: Ground Level
Direction of Observer from Discharge Point:
Southeast
Wind Velocity: 2 to 5
Detached Plume: No
SUMMARY OF AVERAGE OPACITY
Set Number
1
2
3
4
5
6
7
8
9
10
11
12
13
14
15
16
17
18
19
20
Time Opacity
Start End Average
7:30- 7:36 0
** 0
0
0
0
0
0
0
0
0 .
0
0
0
0
0
0
0
0
0
0
Time
Set Number Start End
21
22
23
24
25
26
27
28
29
30
31
32
33
34
35
36
37
38
39
40
Opaci ty
Average
* Two observers made simultaneous readings. The greater of their readings is reported.
** Subsequent sets were each of 6 minutes duration, and there were no time lapses between
sets.
C-44 '
-------
Table C-25, continued.
SKETCH SHOWING HOW OPACITY VARIED WITH TIME:
15
10
234
TIME, hours
C-45
-------
Table C-26
FACILITY C
SUMMARY OF VISIBLE EMISSIONS *
Date: April 10, 1975
Type of Plant: Phosphate Rock Caldner
Type of Discharge: Participate
Location of Discharge: Stack from Scrubber
Height of Point of Discharge: 105 feet
Description of Background: Sky
Description of Sky: Overcast
•Hind Direction: North
Color of Plume: White
Interference of Steam Plume: Yes
Duration of Observation: 3 hours 0 min
Distance from Observer to Discharge Point:
1400 feet
Height of Observation Point: Ground Level
Direction of Observer from Discharge Point:
Southeast
Wind Velocity: 0 to 16
Detached Plume: No
SUMMARY OF AVERAGE OPACITY
Set Number
1
2
3
4
5
6
7
8
9
10
11
12
13
14
15
16
17
18
19
20
Time Qpaci ty
Start End Average
10:45 10;51 0
** ' o
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
Time
Set Number Start End
21
22
23
24
25
26
27
28
29
30
31
32
33
34
35
36
37
38
39
40
Opaci ty
Averaqe
0
' 0
n
u
o
w
o
\J
0
\J
fl
U
* Two observers made simultaneous reaoings. me greater of their readings 1s reported.
** Subsequent sets were each of 6 *toutes duration, and there were no time lapses between
sets.
C-46
-------
15
I 10
U
OJ
m.
> 5
I a
TaWt C-26, continusd.
SKETCH SHOWING HOW OPACITY VARIED WITH TIME:
TIME, hours
C-47
-------
Table C-27
FACILITY F
SUMMARY OF VISIBLE EMISSIONS *
Date: March 25, 1975
Type of Plant: Phosphate Rock Grinder
Type of Discharge: Stack from Baghouse
Location of Discharge: T°P of stack
Height of Point of Discharge: 75 feet
Description of Background: Brown, Rusty Conveyor
Description of Sky: Overcast
Hind Direction: Not Reported
Color of Plume: White
Interference of Steam Plume: No
Duration of Observation: 2 hours 14 min
Distance from Observer to Discharge Point:
50 feet
Height of Observation Point: 85 feet
Direction of Observer from Discharge Point:
East
Wind Velocity: Not Reported
Detached Plume: No
SUMMARY
Set Number
1
2
c*
3
4
5
w
6
w
7
/
8
W
g
10
11
t I
12
13
14
15
16
17
18
19
V J
20
OF AVERAGE OPACITY
Time Opacity
Start End Average
12:30 12:36 0
** ' 0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
SUMMARY OF AVERAGE
Time
Set Number Start End
21
22
23
24
25
26
27
28
29
30
31
32
33
34
35
36
37
38
39
40
OPACITY
Opaci ty
Average
0
* Two observers made simultaneous readings. The greater of their readings is reported.
** Subsequent sets were each of 6 minutes duration, and there were no time lapses between sets
C-48
-------
Table C-27, continued.
15
| 10
!
£ 5
u
i 0
SKETCH SHOWING HOW OPACITY VARIED WITH TIME:
2 3 4
TIME, hours
C-49
-------
Table C-28
FACILITY F
SUMMARY OF VISIBLE EMISSIONS *
Date: March 25, 1975
' Type of Plant: Phosphate Rock Grinder
Type of Discharge: Stack from Baghouse
• Location of Discharge: Top of Stack
Height of Point of Discharge: 75 feet
Description of Background: Brown, Rusty
Description of Sky: Partly Cloudy
•Hind Direction: Northwest
Color of Plume: White
Interference of Steam Plume: No
Duration of Observation: 2 hours 0 min
Distance from Observer to Discharge Point:
50 feet
Height of Observation Point: 90 feet
Conveyor Direction of Observer from Discharge Point:
East
Wind Velocity: 10
Detached Plume: No
SUMMARY OF AVERAGE OPACITY
Set Number
1
7
/
g
10
11
-.11
12
13
14
15
16
17
18
19
20
Time Qpaci ty
Start End Average
5:00 5:06 0
** 0
0
o
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
Time
Set Number Start End
21
22
23
24
25 ,
26
27
28
29
30
31
32
33
34
35
36
37
38
39
40
Ooacitv
Averaae
. Two observers -id. staltaneous readings. The greater of their readings 1s reported.
.« Upsets «« each of 6 »1»Utes .-ration, and there ..re no «.. Upses between
sets.
-------
15
tt
a
Table C-28, continued.
SKETCH SHOWING HOW OPACITY VARIED WITH TIME:
2 3
TIME, hours
C-51
-------
Table C-29
FACILITY F
SUMMARY OF VISIBLE EMISSIONS*
Date: March 26, 1975
Type of Plant: Phosphate Rock Grinder
Type of Discharge: Stack from Baghouse
Location of Discharge: Top of Stack
Height of Point of Discharge: 75 feet
Description of Background: Off-white Building
Description of Sky: Clear
•Wind Direction: Northeast
Color of Plume: White
Interference of Steam Plume: No
Duration of Observation: 2 hours 0 min
SUMMARY OF AVERAGE OPACITY
Distance from Observer to Discharge Point:
50 feet
Height of Observation Point: 85 feet
Direction of Observer from Discharge Point:
East
Wind Velocity: 15 to 25
Detached Plume: No
SUMMARY OF AVERAGE OPACITY
Set Number
1
2
3
w
4
5
6
7
8
9
•TO
n
13
14-
15
16
17
18
19
20
Time Opacity
Start End Average
11:00 11:06 0
** . 0
0
0
0
0
0
0
0
0
0
o
0
0
0
0
0
0
0
0
Time
Set Number Start End
21
22
23
24
25
26
27
28
29
30
31
32
33
34
35
36
37
38
39
40
Opaci ty
Average
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
* Two observers made simultaneous readings. The greater of their readings is reported.
** Subsequent sets were each of 6 minutes duration, and there were no time lapses between
sets.
C-52
-------
T«We C-29, continued.
15
S
a.
i o
SKETCH SHOWING HOW OPACITY VARIED WITH TIME:
2 3
TIME, hours
C-53
-------
Table C-30
FACILITY 6
SUMMARY OF VISIBLE EMISSIONS *
Date: April 5, 1975
Type of Plant: Phosphate Rick Grinder
Type of Discharge: Particulate
- Location of Discharge: *«* f™ Ba9house
Height of Point of Discharge: 46 feet
Description of Background: Dark Building
Description of Sky: Overcast
Wind Direction: South
Color of Plume: None
Interference of Steam Plume: No
Duration of Observation: 3 hours 0 min
Tim? Opacity ,.._,,. £
Set Number
1
3
4
8
10
n
12
13
14
15
16
17
18
19
20 '
Start End Averaqe
4:00 4:06 0
** • o
o
0
0
0
0
o
0
0
0
0
0
0
0
0
0
0
0
0
Set Number Start
21
22
23
24
25
26
27
28
29
30
31
32
33
34
35
36
37
38
39
40
Distance from Observer to Discharge Point:
270 feet
Height of Observation Pdlnt: Around Level
Direction of Observer from Discharge Point:
East
Wind Velocity: 4 to 20
Detached Plume: No
SUMMARY OF AVERAGE OPACITY
Opacity
0
0
0
0
0
0
0
0
0
0
* Two observers made simultaneous readings. The greater el their readings is reported.
** Subsequent sets were each of 6 minutes duration, and there was a 16 minute lapse
(6:44 to 7:00) in readings during a plant malfunction.
C-54
-------
Tablo C-30, continued.
SKETCH SHOWING HOW OPACITY VARIED WITH TIME:
15
1 10
I
> 5
2 3
TIME, hours
C-55
-------
Table C-31
FACILITY 6
SUMMARY OF VISIBLE EMISSIONS *
Date: April 7, 1975
Type of Plant: Phosphate Rock Grinder
Type of Discharge: Participate
Location of Discharge: Duct from Baghouse
Height of Point of Discharge: 46 feet
Description of Background: Dark Building
Description of Sky: Overcast
•Mind Direction: Korthwest
Color of Plume: None
Interference of Steam Plume: No
Duration of Observation: 3 hours 20 min
SUMMARY OF AVERAGE OPACITY
Set Number
1 '
2
3
4
S
6
7
8
9
10
11
12
13
14
15
16
T7
18
19
20
Time Opacity
start End Average
9:25 9:31 0
** 0
0
0
w
n
u
n
\j
o
o
0
0
o
\J
n
V
0
o
V
0
V
n
\J
n
\j
o
\J
o
w
0
.
Set Nun
21
22
23
24
25
26
27
28
29
30
31
32
33
34
35
36
37
38
39
40
Distance from Observer to Discharge Point:
270 feet
Height of Observation Point: Ground Level
Direction of Observer from Discharge Point:
East
Wind Velocity: 7 to 15
Detached Plume: No
SUMMARY OF AVERAGE OPACITY,
Time Opacity
s»t Number Start End, Average
0
0
•o
0
0
0
0
0
0
0
0
0
,.„,
C-56
-------
Table C-31, continued.
15
s 10
o •
I 0
. SKETCH SHOWING HOW OPACITY VARIED WITH TIME:
2 34
TIME, hours
C-57
-------
Table C-32
FACILITY 6
SUMMARY OF VISIBLE EMISSIONS *
Date: April 7, 1975
Type of Plant: Phosphate Rock Grinder
Type of Discharge: Participate
> Location of Discharge: Duct from Baghouse
Height of Point of Discharge: 46 feet
Description of Background: Dark Building
Description of Sky: Overcast
Hind Direction: Northwest
Color of Plume: None
Interference of Steam Plume: No
Duration of Observation: 3 hours 20 min
Distance from Observer to Discharge Point:
275 feet
Height of Observation Point: Ground Level
Direction of Observer from Discharge Point:
Northeast
Wind Velocity: 5 to 13
Detached Plume: No
SUMMARY OF AVERAGE OPACITY
Opacity
sunriHf
Set Number
1
•3
«j
A
T
c
3
£
o
7
8
9
10
11
12
13
14
15
16
17
18
10
t y
20
Time Opacity
Start End Averaqe
3:20 3:26 0
** • 0
fl
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
Time
Set Number Start End
21
22
23
24
25
26
27
28
29
30
31
32
33
34
35
36
37
38
39
40
Average
0
0
0
0
0
'0
0
0
0
0
0
0
* Two observers made simultaneous readings. The greater of their readings is reported.
** Subsequent sets were each of 6 minutes duration, and visible emissions measurements were
curtailed for twenty minutes (from 5:51 to 6:11) during a plant malfunction.
C-58
-------
Table C-32, continued.
15
£ 10
u
SKETCH SHOWING HOW OPACITY VARIED WITH TIME:
2 3
TIME, hours
C-59
-------
Table C-33
FACILITY H.
SUMMARY OF VISIBLE EMISSIONS *
Date: March 26, 1975
Type of PIant: Materials Hand! 1ng
Type of Discharge: Particulate
. Location of Discharge: Baghouse Stack
Height of Point of Discharge: ISO feet
Description of Background: Green Trees
Description of Sky: Clear
Hind Direction: Northeast
Color of Plume: White
Interference of Steam Plume: No
Distance from Observer to Discharge Point:
75 feet
Height of Observation Point: 150 feet
Direction of Observer from Discharge Point:
South-Southwest
Mind Velocity: 5
Detached Plume: No
UUrauiuu ui uu:
SUMMARY
Set Number
1
3
6
8
9
10
n
12
13
14
15
16
17
18
19
20
nF AVERAGE OPACITY _
Time Ooacity
Start End Averaqe
3:00 3:06 0
** ' 0
n
w
0
0
o
V
0
o
w
o
o
\f
0
\J
o
w
o
\J
n
w
n
w
n
w
n
\j
n
\j
n
V
n
u
SUMMARY OF AVERAGE OPACITY
Set Number Start ^d ' Averaqe
• 21
22
23
24
25
26
27
28
29
30
31
32
33
34
35
36
37
38
39
40
-
-
between
C-60
-------
TaWe C-33, continued.
SKETCH SHOWING HOW OPACITY VARIED WITH TIME:
15
10
s
0
2 3
TIME, hours
C-b'I
-------
Table C-34
FACILITY I
SUMMARY OF VISIBLE EMISSIONS *
Date: March 25, 1975
Type of Plant: P™und rock transfer
Type of Discharge: Stack from baghouse
• Location of Discharge: Top of stack
Height of Point of Discharge: 100 feet
Description of Background: Dark gray overcast
Description of Sky: Overcast
-Wind, Direction: West
to!or of Plume: Wnite
Interference of Steam Plume: No
Duration of Observation: 1 hour, 0 minutes
Distance from Observer to Discharge Point:
300 feet
Height of Observation Point: 30 feet
Direction of Observer from Discharge Point:
North
Wind Velocity: 10
Detached Plume: No .
SUMMAF
Set Number
1
3
4
5
p.
7
a
g
10
11
12
13
14
15
is
17
IB
19
20
Time Opacity
Start End Average
3:17 3.:23 0
** 0
0
0
0
0
0
. 0
0
0
Time Opacity
Set Number Start End Average
21
22
23
25
26
27
28
29
30
31
. 32
33
34
35
36
37
38
39
40
*Two observers made simultaneous readings. The greater of
Subsequent sets were each of 6-minutes duration, and there were
sets .
{* een
lapses between
C-62
-------
Table C-34, continued.
SKETCH SHOWING HOW OPACITY VARIED WITH TIME:
15
10
5
0
2 3
TIME, hours
C-63
-------
Table C-35
FACILITY J
SUMMARY OF VISIBLE EMISSIONS *
Date: March 25, 1975
Type of Plant: Ground rock transfer
Type of Discharge: Stack from baghouse
. Location of Discharge:T°P of stack
Height of Point of Discharge: 12° feet
Description of Background: Gray sk^
Description of Sky: Overcast
'Hind Direction: Northwest
Color of Plume: White
Interference of Steam Plume: ;^°
Duration of Observation: 1 hour, 0 minutes
Distance from Observer to Discharge Point:
150 feet
Height of Observation Point: 75 feet
Direction of Observer from Discharge Point:
Nortnwest
Wind Velocity: 10
Detached Plume: H
SUMMARY OF AVERAGE OPACITY
Set Number
1
2
3
4
~
5
6
7
1
8
9
10
n
12
13
14
15
16
17
18
19
20
Time Ooacitv
Start End Averaqe
4:45 4:51 0
** 0
0
a
0
0
0
0
0
0
0 '
Time Ooacitv
Set Number Start End Averaae .
21
22
23
24
25
26
27
28
29
30
31
32
33
A ft
34
35
36
37
38
39
40
*Two observers made simultaneous readings. The greater of their readings is reported.
**Subsequent sets were each of 6-minutes duration, and there were no time lapses between
sets. . .
C-64
-------
Table C-35, continued.
SKETCH SHOWING HOW OPACITY VARIED WITH TIME:
15
| 10
Oi
a.
I 5
1 o
2 3
TIME, hours
C-65
-------
TABLE C-36
FACILITY K
Summary of Visible Emissions
Date: June 22, 1976
Type of Plant: Phosphate rock calciner
Type of Discharge: Stack from scrubber
Location of Discharge: Top of stack
Height of Point of Discharge: 150 feet
Description of Background: Sky
Description of Sky: Partly cloudy
Wind Direction: Northeast
Color of Plume: White
Duration of Observation: 1 hour 0 minutes
SUMMARY OF AVERAGE OPACITY
Distance from Observer to Discharge Point:
200 yards
Height of Observation Point: Ground level
Direction of Observer from Discharge Point:
Northwest
Wind Velocity: 15-20 MPH
Detached Plume: Yes
/
- SUMMARY OF AVERAGE OPACITY
Time
Set Number Start End
1 2:00 2:06
2 *
3
4
5
6
7
8
9
10
11
12
13
14
15
16
17
18
19
20
Opacity
Average
0.83
0
0
0
0
0
0
0
0
0
Time Opacity
Set Number Start End Average
21
22
23
24
•"" 25
26
27
28
29
30
31
32
33
34
35
36
37
38
39
40
* Subsequent sets were each of 6 minutes duration, and. there were no time lapses between sets.
C-66
-------
Tiblt C-36, continued.
SKETCH SHOWING HOW OPACITY VARIED WITH TIME:
15
10
5
2 3
TIME, hours
C-67
-------
-------
APPENDIX D. EMISSION MEASUREMENT AND CONTINUOUS MONITORING
D.I Emission' Measurement Mathods
For the phosphate rock processing industry, the Environmental Protection
Agency relied on Method 5 for measuring particulate emissions, Method 9 for
measuring visible emissions, and Method 138 for fluoride emissions. These
methods were used as described in Appendix A of 40 CFR Part 60 and published
1n the Federal Register (December 23, 1971 and October 23, 1974).
The particulate mass catches from these process emissions were relatively
low, especially for the baghouse controlled emissions. The mass catch amounts
ranged from about 12 mg to over 300 mg. For the particularly low concentra-
tions, some tests were extended to over 3 hours in an effort, to obtain
accurately measurable catches. In-house tests have shown that acceptable
accuracy (j^ 10/0 can be obtained with a minimum catch of 25 mg. Most of the
inaccuracy at this level and lower is found on the high side of the measure-
ment; that is, somewhat more mass is measured than is actually collected.
Visible emission readings were made difficult because of high moisture
content of scrubber exhausts from several of the processes. In most cases,
opacity readings were made at the leading edge of the steam plume.
D.2 Continuous Monitoring
Effluent gas from the phosphate rock processes are not excessively hot
(less than 121° C or 250°F),faut can contain fluorides that may react
with water to form acids that would etch, glass materials. Glass lenses
on opacity monitoring equipment should either be protected from fluoride
deposits or replaced with material not subject to etching. Visible emission
D-l
-------
monitors are covered by EPA performance standards contained is Appendix B
«
of 40 CFR Part 60 (Federal Register. September 11, 1974).
Equipment and installation costs are estimated to be $18,000 to $20,000
and annual operating costs, including data recording and reduction, are
estimated at $8,000 to $9,000.
D.3 Performance Test Methods
The performance test method recommended for particulate matter is
Method 5. Because of the construction of some control equipment, special
stack extensions may be required to obtain acceptable sampling conditions.
;
Low particulate concentrations in the stack gases from fabric collectors
necessitate longer sampling times and larger sample volumes. The recommended
minimum sampling volume is 4.5 dsm3 (160 dscf). Commercially available high
volume sampling trains conforming to Method 5 specifications would allow tests
of shorter duration while obtaining the minimum sample volume, thus reducing
time and expense of tests.
Sampling costs for a test consisting of 3 particulate runs is estimated
to be about $5,000 to $9,000. This estimation is based on the sampling site
modifications such as ports, scaffolding, ladders, and extensions costing
from $2,000 to $4,000 and testing being conducted by contractors. If in-plant
personnel are used to conduct the tests, the costs will be somewhat less.
Method 9 is recommended for visible emissions.
D-2
-------
APPENDIX E. ENFORCEMENT ASPECTS
E.I. GENERAL
The recommended standards of performance will limit emissions
of particulates and visible emissions from phosphate rock dryers,
calciners, grinders and ground rock transfer systems at phosphate rock
Plants. The control systems which can be installed to comply with these
standards are scrubbers, fabric filters, electrostatic precipitators, or
a combination of these. The control system may serve one or several
affected facilities simultaneously. Aspects of enforcing these standards
are discussed below for each affected facility.
E.2. DRYERS
Factors affecting the level of uncontrolled emissions from phosphate
rock dryers include the design and operation of the dryer and the type of
rock being dried. The effect of process design and operation on uncontrolled
ennssions is discussed in Chapter 3. The operator usually has little control
over the design of the dryer after it is installed, and operation during:a
compliance test should be no.different than the way the process is normally
operated. The compliance test should be performed while the dryer is opera-
ting at the maximum production rate at which it is expected to run in
the future, which may be greater than design parameters indicate. As stated
1n the facility descriptions in Appendix C, dryers are designed for a
certain degree of moisture removal, and production at this moisture removal
E-l
-------
rate will be a function of the characteristics of the feed to the dryer.
Generally, production throughput at a constant moisture removal rate
will be greater for small, dry feed than for large, wet feed. The.
enforcement official should therefore be more concerned with the heat
Input (fuel addition rate) to the dryer than the production throughput.
*
Some dryers are designed to bum more than one type of fuel (i.e.,
natural gas or fuel oil). In these cases, emissions from the dryer
should be sampled while the dryer is burning the dirtiest fuel it will
burn in the future. An exception to this would occur if the dryer is
designed to burn one fuel, such as natural gas, during normal operation,
but can use an alternate fuel, such as fuel oil, when the cleaner fuel
'is not available. In these cases, the dryer should be tested during
normal conditions (e.g., burning natural gas). What is "normal" is
somewhat subjective and should be determined by the enforcing agency.
The type of rock being processed by the dryer may affect emissions
from some dryers processing rock from the Florida deposits. The Florida
rock falls into two calssifications, pebble rock and concentrates. Most
operators indicate that they experience greater particulate emissions
when drying pebble rock than when drying concentrates. The reason
they give is that the pebble rock goes through fewer washings in the
beneficiation process (see Chapter 3) and, therefore, has more clay
adhering to its surface. Attrition in the dryer causes submicron-sized
E-2
-------
clay particles to be sloughed off, resulting 1n greater emissions to
the control system. Because of this, at least half of the rock being
processed during the performance tests .should be pebble rock. Of
t ' .
course, if pebble rock will never be processed in the dryer, this
requirement should be waived.
E.3. CALCINERS
The enforcement aspects for calciners are the same as those
presented above for dryers. The only-noteworthy difference is that it
is unlikely that any units will be built to calcine Florida rock, so
the type of raw material fed to the calciner need not concern the
enforcement official.
.E.4. GRINDERS
Phosphate rock grinders are of two basic designs: ball mills and
roller milis. Ball mills are usually ducted to a "single control device;
however, roller mills are frequently operated in parallel with several
ducted to one control device. Therefore, it is incumbent on the enforcement
official to be certain that all mills ducted to the control device are
operating during the compliance tests. Types of raw materials do not
affect emissions from phosphate rock grinders.
Factors which affect production rate from phosphate rock grinders
are the mesh size (fineness) of the grind and the design of the grinder.
Generally, emissions per ton of production will increase as the rock is
ground to smaller mesh sizes. To increase the fineness of the grind,
the operator must increase the residence time of the rock in the grinder,
biasing the particle size distribution toward the smaller sizes. However,
E-3
-------
the process which will ultimately use the ground rock has been designed
to accept a certain size rock, typically 60 percent through 200 mesh,
*
and operates most efficiently with that size of rock. Therefore,
fineness of the grind is not generally a parameter which the operator
changes frequently. As with dryers and calciners, production throughput
of grinders is incidental to other considerations. Production tonnage
decreases as the mesh size being produced gets smaller. Once the
product size is set, the operator usually monitors the amperage of
the mill motor and/or mill fan and runs the grinding mill at the
maximum production possible without damaging the equipment. The enforce-
ment official should obtain these maximum tolerances from previous
•operating data (usually available from past log sheets) or, if necessary,
from design data.
E.5. GROUND ROCK HANDLING SYSTEMS
The ground rock handling standard is unique in that it only regu-
lates visible emissions. Also, because the ground rock handling system
usually operates intermittently, the visible emissions test must be
scheduled when the system will be operated for the duration of the
observations.
E-4
-------
APPENDIX F. THE STACK GAS DISPERSION MODEL
F.I. DESCRIPTION OF THE SINGLE SOURCE MODEL CJMHCRD-1)
The model used to estimate ambient concentrations for the phosphate
rock processing plant is one developed by the Meteorology Laboratory, EPA.
This model is designed to estimate concentrations due to sources at a single
location for averaging times from one hour to one year.
This model is a Gaussian plume model using diffusion coefficients
suggested by Turner (1970).* Concentrations are calculated for each hour
of the year, from observations of wind direction (in increments of 10 degrees),
wind speed, mixing height, and atmospheric stability. The atmospheric
stability is derived by the Pasquill classification method as described by
Turner (1970). In the application of this model, all pollutants are con-
sidered to display the dispersion behaviour of non-reactive gases.
Meteorological data for 1964 are used as input to the model. The reasons
for this choice are: (1) data from earlier years did not have sufficient
resolution in the wind direction! and (2) data from subsequent years are
readily available on magnetic tape only for every third hour.
*Turner, D. B., "Workbook of Atmospheric Dispersion Estimates," U.S
Dept. of H.E.W., PHS Publication No. 999-Ap-24 (Revised 1970).
F-l
-------
Mtxtng height data are obtained from the twice-a-day upper air observa-
tions made at the most representative upper air station. Hourly mixing heights
are estimated By the model using an objective interpolation schemed
A feature of this model ts the modification of plume behavior to
account for aerodynamic effects -for plants in which the design is not optimal
(see Appendix B). Another important aspect of the model ts the ability to
add concentrations from stacks located closely together. In this feature,
no consideration is gtven to the physical separation between the stacks
since all are assumed to be located at the same geographical point.
Calculations are made for 180 receptors', (at 36 azimuths and five selectable
distances from the source). The OMHCRD-1 model used here can consider both
diurnal and seasonal variations in the source. Separate variation factors can
be applied on a monthly basis to account for seasonal fluctuations and on an
hourly basis to account for diurnal variations. Another feature of the model
Is the ability .to compute frequency distributions for concentrations of any
averaging period over the course of a year. Percentages of various ranges in
pollutant concentrations are calculated.
F.2. AERODYNAMIC-EFFECTS .'MODIFICATION -OF THE SINGLE SOURCE MODEL
Note: The aerodynami c- effects version is a more general form of ^e single
source model. All remarks made in section F.I apply equally to either
version.
' The single, source model does not address the aerodynamic complications
which arise when plant design is less than ideal. These effects result from
the interaction of the wind with the physical structure of the plant. Such
interaction can retard or, in the extreme, prevent plume rise. The extreme
F-2
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case is coranonly referred to as ''downwash." With downwash, the effluent is
brought downward into the wake of the plant, from which point it diffuses as
though emitted very close to the ground. In the retardation case, some of
the dispersive benefits of plume rise are lost; while in the downwash case,
all of the benefits of plume rise are lost, along with most of the benefits
of stack elevation. Both phenomena-but especially downwash-can seriously
increase the resulting' ambient air impact.
The aerodynamic-effects modification, then, is an attempt to include
these effects in a predictive model. It was developed within EPA and, while
not yet validated, is the best-known operational approach. Basically, it
enables the model to make an hour-by-hour, stack-by-stack assessment of
the extent (if any) of aerodynamic complications. The parameters used in
making the assessment are wind spaed, stack gas exit velocity, stack height,
stack diameter, and building height. If a particular assessment indicates no
aerodynamic effect, then for that stack for that hour, the model behaves just
like the unmodified version. If there are aerodynamic effects, the modified
version contains equations fay which the impact of these effects on ground-
level concentrations is estimated.
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APPENDIX 6. CONVERSION FROM ENGLISH TO METRIC UNITS
To convert from
Acre (ac)
British Thermal Unit
(Btu) .
Cubic Foot (ft3)
Degree Farenheit (°F)
Gallon (G)
Grains per Actual
Cubic Foot (Gr/ACF)
Grains per Dry Standard
Cubic Foot (gr/dscf)
Inch of Water (Pressure)
Pound (Ib)
Square Foot (ft2)
Ton (T)
Ton per Hour (TPH)
to
Square Meter (m2)
Joule (J)
Cubic Meter (m3)
Degree Celsius (°C)
Cubic Meter (m3)
Milligrams per Actual
Cubic Meter (mg/m3)
Milligrams per Dry
Standard Cubic Meter
(mg/dsm3)
Pascal (Pa)
Kilogram
Square Meter (m2)
Kilogram (kg)
Kilogram per Second
(kg/s)
Multiply by
, 4.047 x 103
1.055 x 103
2.832 x 10-2
°C = (°F - 32J/1.8
*>
3.785 x 10-3
2.288 x 1Q3
2.288 x 103
2.488 x 102
4.536 x 10-1
9.290 x 10-2
9.072 x 102
2.520 x 10-1
G-l
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(EXAMPLE)
TECHNICAL REPORT DATA
(Piuue read Instructions on the reverse before completing;
2.
1. REPORT NO.
EPA-450/3-79-017
4. TITLE AND SUBTITLE
Phosphate Rock Plants - Background Information: Volume
1, Proposed Standards.
6. PERFORMING ORGANIZATION CODE
r. AUTHOR^)
8. PERFORMING ORGANIZATION REPORT NO.
9. PERFORMING ORGANIZATION NAME AND ADDRESS
Office of Air Quality Planning and Standards
Environmental Protection Agency
Research Triangle Park, North Carolina 27711
12.SPONSORING AGENCY NAME AND ADDRESS
DAA for Air Quality Planning and Standards
Office of Air, Noise and Radiation
U. S. Environmental Protection Agency
Research Triangle Park. North Carolina 27711
3. RECIPIENT'S ACCESSION NO.
i. R£POR.T DATE
September 1979
10. PROGRAM ELEMENT NO.
11. CONTRACT/GRANT NO."
68-02-3063
13 TYPE OF REPORT AND PERIOD COVERED
Draft
TSTSPONSOHING AGENCY CODE
15. SUPPLEMENTARY NOTES
•J6. ABSTRACT
Standards of Performance for the control of emissions from phosphate rock plants are
being proposed under the authority of Section 111 of the Clean Air Act. These stan-
dard! would apply to new, modified, and reconstructed phosphate rock dryers, calcners,
grinders, and ground rock handling systems, and would limit emissions of Pjrticulate
matter by 85 to 98 percent below the levels permitted by current typical state regu-
lations. This document contains background information, environmental and economic
impact assessments, and the rationale for the proposed standards... Volume•«-"»»«
will be published when the standards are promulgated, will contain a summary of the
public comments on the proposed standard and EPA's responses. A discussion of any
differences between the proposed and promulgated standards will also be included.
=
KEY WORDS AND DOCUMENT ANALYSIS
DESCRIPTORS
b.lOeNTIFIEHS/OPEN ENDED TERMS
c. COSATI Field/Group
Air pollution
Pollution control
Standards of performance
Phosphate rock plants
Particulate matter
Air Pollution Control
J18. DISTRIBUTION STATEMENT
Jnlimited
19. SECURITY CLASS (This Report I
Unclassified
21. NO. OF PAGES
20. SECURITY CLASS iThispage)
Unclassified
22. PRICE
EPA F«m 2220-UR«v. 4-77) MCVIOUS COITION is «»,„«„
.S. GOVERNMENT PRINTING OFFICE: 1979 -640-01* 3942REGION NO. 4
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