United States
Environmental Protection
Agency
Solid Waste and
Emergency Response
(OS-305)
EPA 530-F-92-026
October 1992
Office of Solid Waste
f/EPA Environmental
Fact Sheet
EPA Revises Quality Assurance Measures
For The Toxicity Characteristic Leaching
Procedure
This rule amends the requirements for sample testing associated
with the Toxicity Characteristic Leaching Procedure CTCLP). By
removing "spike recovery correction" from the Ust of required quality
assurance measures, the TC testing methods will remain consistent
with those outlined in EPA's manual on RCRA testing methodology.
Background
Subtitle C of the Resource Conservation and Recovery Act (RCRA)
creates a comprehensive program for the safe management of hazardous
waste. Under this program, EPA has promulgated criteria for identifying and
listing hazardous wastes, along with standards for the storage, treatment
and disposal of those wastes. The guidance document, Test Methods For
Evaluating Solid Waste, Physical/Chemical Methods, SW-846, was first
published in 1980 to support the associated testing requirements.
On February 8, 1990, the
Agency requested comment on
proposed revisions to Chapter
One of the RCRA methods manual.
The revisions included specific
mandatory quality assurance
procedures for all testing conducted
pursuant to Subtitle C of RCRA,
and identified "spike recovery
correction" (see box) as a Quality
Assurance (QA) requirement.
On March 29, 1990, EPA
revised the existing Toxicity
Characteristic fTC) and replaced the
Extraction Procedure (EP) Toxicity
Characteristic Test, with the TCLP.
On June 29, 1990, the Agency
Spike Recovery Correction
is a procedure used to document
the bias of a method in a given
sample matrix. A known
concentration of a target analyte
is added to the sample prior to
analysis. Then, during the
analysis, the percentage of
the target analyte detected is
measured. If the analysis detects
less than 100 percent of the target
analyte, then the concentration of
that analyte and other similar
chemicals present in the sample
can be adjusted by that
percentage.
-------
United States
Environmental Protection
Agency
Solid Waste and
Emergency Response
(OS-305)
EPA530-F-92-026
October 1992
Office of Solid Waste
?/EPA Environmental
Fact Sheet
EPA Revises Quality Assurance Measures
For The Toxicity Characteristic Leaching
Procedure
This rule amends the requirements for sample testing associated
with the Toxicity Characteristic Leaching Procedure (TCLP). By
removing "spike recovery correction" from the list of required quality
assurance measures, the TC testing methods will remain consistent
with those outlined in EPA's manual on RCRA testing methodology.
Background
Subtitle C of the Resource Conservation and Recovery Act (RCRA)
creates a comprehensive program for the safe management of hazardous
waste. Under this program, EPA has promulgated criteria for identifying and
listing hazardous wastes, along with standards for the storage, treatment
and disposal of those wastes. The guidance document, Test Methods For
Evaluating Solid Waste, Physical/Chemical Methods, SW-846, was first
published in 1980 to support the associated testing requirements.
On February 8, 1990, the
Agency requested comment on
proposed revisions to Chapter
One of the RCRA methods manual.
The revisions included specific
mandatory quality assurance
procedures for all testing conducted
pursuant to Subtitle C of RCRA,
and identified "spike recovery
correction" (see box) as a Quality
Assurance (QA) requirement.
On March 29, 1990, EPA
revised the existing Toxicity
Characteristic fTC) and replaced the
Extraction Procedure (EP) Toxicity
Characteristic Test, with the TCLP.
On June 29, 1990, the Agency
Spike Recovery Correction
is a procedure used to document
the bias of a method in a given
sample matrix. A known
concentration of a target analyte
is added to the sample prior to
analysis. Then, during the
analysis, the percentage of
the target analyte detected is
measured. If the analysis detects
less than 100 percent of the target
analyte, then the concentration of
that analyte and other similar
chemicals present in the sample
can be adjusted by that
percentage.
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