Tuesday
 January 3, 1995
 Part V
Protection  Agency
40 CFR Part 268
Land Disposal Restrictions Phase II—
Universal Treatment Standards, and
Treatment Standards for Organic toxicity
Characteristic Wastes and Newly Listed
Wastes; Final Rule  ,         :

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242-*•'.",. ;~F£deral;Tlegiste"rX Vol...60,>No.. I,./..Tuesday..January,3,
                                                                                     . and.;Rqgulatipns
  ENVIRONMENTAL PROTECTION
  AGENCY             •     '

  40 CFR Part 268     •

  [FRU-S129-2] •     ;   ' -     •    .

' Land Disposal Restrictions Phase II-
  Universai Treatment Standards, and
  Treatment Standards for Organic
  Toxiclty Characteristic Wastes and
  Newly Listed Wastes

  AGENCY: Environmental Protection
  Agency (EPA).
  ACTION: Final rule; technical
  amendments.	•	•   -  ,.'

  SUMMARY: On September 19,1994, EPA
  published regulations promulgating
  congrossionally-mandated prohibitions '
  on land disposal of certain hazardous •
  \vnstes. This notice corrects errors and
  clarifies the language in the preamble
  and regulation of the September 19,
  1994 final rule.
  EFFECTIVE DATE: This rule is effective on
  December 19,1994.
  ADDRESSES: Copies of the rule can be
  obtained from the RCRA Docket .(5305),
  U.S. Environmental Protection Agency,
  Room 2610,401 M Street, S.W.,
  •Washington, B.C. 204GO. The RCRA
  Docket is open from 9:00 am to 4:00 pm
  Monday through Friday, except for
  federal holidays. The public must make
  tin appointment to review docket
  materials by calling (202) 200-9327. The
• public may copy a maximum of 100
  pages from any regulatory document at
  no cost. Additional copies cost S0.15
  per page.'
  FOR FURTHER INFORMATION CONTACT: For
  general information contact the RCRA
  Hotline at (800) 424-9346 (toll free) or
  (703) 920-9810 in the Washington, DC •
  metropolitan area. Far technical
  information coritact-Doug Heimlich   .
   (5302\V). Office of Solid Wasto, 401 M
   Street, S.W., Washington, DC 20460,
   (703)308-8489.               .   ,
   SUPPLEMENTARY INFORMATION:
   1 Reasons and Basis for Today's Amendment
   II Amendments to the Phase II Final Rule
    .A Section 268 2
     D Section 2687»
     C Seutlon 268 9             .
  .   D Section 268.40      '     .
     E Section 268 42                •
    =' F Section 268.48
     G. Appendix X to Part 268
    III. Glorification of Issues
     A State Authority Policy for Universal
       Treatment Standards
     U. Flowchart Clarification
    IV Rationale for Immediate Effective Date ,
    V R.'jjuljtory Impact Analysis
                                      I. Reasons and Basis for Today's
                                      Amendment  "   •   • .   .      -..-...
                                      •  The Agency has received comments,.
                                      from the regulated community and.State
                                      agencies requesting clarification on .  .
                                      certain aspects of the September 19,
                                      1994 Phase II final rule' (59 FR 47982).  >.
                                      Today's amendment responds to these
                                      comments.    .  *  .- •    •  ..';•"'
                                      II. Amendments to the Phase II Final
                                      Rule          '.     '  '....  " '  •"    ':
                                      A. Section 268.2     .    '
                                       -Like zinc, vanadium is not considered
                                      to be an "underlying hazardous   •..
                                      constituent" in characteristic wastes. In
                                      the definition of underlying hazardous
                                      constituent at 268.2(i), vanadium was  •'
                                      inadvertently left out as an exception to
                                      the definition. It is being placed as an
                                      exception in the definition at 268.2(i) in
                                      today's amendment.

                                      B. Section 268.7   '    '  ,';•
                                         In the preamble of the Phase II final ..
                                      rule, EPA stated that, as a simplifying '
                                      measure, it was amending the LDR .
                                      -notification requirements to minimize ,
                                      the amount of information that must be
                                       placed 'on the LDR notification in .
                                       certain circumstances (see 59 FR 48004).
                                       Prior to promulgation of the Phase II
                                       rule, the hazardous constituents in
                                       F001-F005 spent solvents, F039, wastes
                                       subject to the California list provisions
                                       of § 268.32 or RCRA section 3004(d),
                                       and underlying.hazardous constituents '
                                       in certain characteristic wastes had to be
                                       listed on the LDR notification. In Phase
                                       II, this language was .changed sojthat if
                                       the generator/treater monitors for. all  the
                                       hazardous constituents in F001-F005
                                       spent solvents, F039, and underlying
                                       hazardous constituents in certain
                                       characteristic wastes, then there would.
                                       be no need to list any of the constituents
                                       on the LDR notification. If, however, the
                                       generator/treater is monitoring for a
                                       subset of these constituents, the subset.
                                      • of constituents in the-ivaste (or, in the. .
                                      ' case of .underlying hazardous.
                                      ' constituents in certain characteristic   •
                                       wastes, the ones reasonably expected to
                                       be present at point of generation) would
                                       be required to be listed on the LDR .
                                       notification. In making this change, EPA
                                       inadvertently left outlanguage in
                                        §§268.7(a)(l)(ii),268.7(a)(2XiKB),.and. .
                                        268.7(b)(4)(ii) applying this provision to
                                        California list wastes prohibited-' ...
                                        pursuant to § 268.32 or RCRA section
                                        3004(d). A reference to these California
                                        list wastes is therefore being added to ,
                                        the sections mentioned above in today's
                                        amendment.       '.-   •  •.-.',
                                       '  An error"was also found in   ' .   ••
                                        § 268.7(a)(l). In this section, EPA    '
                                        explained that before the Phase II final
 rule a generator managing a restricted  .  • •
 waste that did not meet the applicable;,,'
 treatment standards set 'forth in Siibpart  ;
 D of Part 268, or exceeds the prohibition
 levels set forth in § 268.32 or RCRA  ';.'
 section 30Q4(d), was required, with each  '
 .shipment-of waste, to notify the   . / : •  .
 treatment or storage facility in writing of  ,
 the appropriate treatment standards set.
 forth in Subpart D of this -part and any
 applicable .prohibition levels set forth in
 § 268.32 or RCRA section 3004(d)..
•  As explained on page 48004 of the
 Phase II preamble, EPA dropped the-
 requirement to include, the .treatment. • -
 standard or the reference to the   "  •
 treatment standard on the LDR    ,  -
 notification. EPA-overlooked,the   .
 regulatory language above (in italics) .
 when modifications were made in the
 .Phase II rule. Thus it is being removed.,
 in this technical amendment. The   . • .   •
 statement is changed to read, ."*' •*" -*   '.
. notify the treatment or storage facility in
 writing.'".  '•.       •'        ' ,'•   • .. ;:
   Another error was made in   •'• . - '•—:.. •..
 § 268.7(a)(l). Paragraph (v) should have .
 been redesignated as paragraph (vi), and .
 a new paragraph (y) added.'Although
 paragraph (v) was revised with the new; .
 language; the existing language that, •,   •
 should have been included in paragraph
 (vi).was inadvertently deleted,- •
 ' Paragraph (vi), with the language that
 appeared as paragraph (v) before the
 Phase  II rule, is being added in today's
 amendments. Also, in order for the new
 paragraph to read properly, paragraph
  (iv) was changed t& delete the final  .
 , word "and," and paragraph (v) was
  changed to add the word, '.'and" at th.6
  end.    •'•:'•'•:   •  '• •'••"• -.'  '.  '<
   , The same error described in the •_• .
  previous paragraph was also made in •
 § 268.7(a)(3): paragraph (vi) should have
  been redesignated as paragraph', (vii), .
  and a  new paragraph (vi) added.   ,:  j
  Paragraph (vii), with the language that _
  appeared as paragraph (vi) before the
  Phase II rule, is.beingTeiri'serted today   .
 ' Also,  paragraph (a)(3)(vi) is being \.  .-
  revised today because it'ha'd been ' f •' :.
 ' merely reproduced (incorrectly) from'
 , paragraph"(a)(l)(v).' -.,.. '-. - -'""•-.   ••
    Jn addition, in § 268.7(a)(8), EPA .
  modified the alternative'treatment '• .
 .  standards for lab packs from identifying
   the wastes that can be included in lab ,
   packs to specifying those wastes that are
   prohibited from being place'd.in lab..'
   packs. EPA made this change in order
   to simplify and clarify this provision.  -
 '  The certification language required :   • • •
   under this section is being changed in
   this technical amendment to say that the
   lab pack "contains only wastes which'
 '  have  not been'exchided under appendix
 .  IV to 40 CFR part 268.'"-The certification
   language that reads "or.solid wastes not

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    , subject to regulation under 40 CFR part
     261" is being removed and is no longer
     considered necessary, because the   ,
     regulated community has in appendix
     IV a list of wastes that are prohibited "
     from placement in a lab pack, the
     Agency believes that deleting this
    'statement is not a substantive change,
     but rather alleviates unnecessary
     language.
       Finally, in the introductory paragraph
     'f § 268.7(d) and in § 268.7(d)(l),.
       tJ 	— — - - \»J u**u il* g f*W,/ {*-LJ\*-Jt
    - generators or treaters who claim an
     exemption for hazardous debris from
 .   • the definition of hazardous waste under
     § 261,3 (e) are subject to notification and
     certification requirements that, •
 -    previously, were to be submitted to the
  -   "Director or authorized State." EPA   '
     recognizes that this designation is •
  .   vague, and is specifying in today's
     amendment that the notification and  ,
  .  certification requirements of § 268.7(d)
    be submitted to.the-Regional .
    Administrator (or his designated
    representative) or. State authorized to
    implement Part 268 requirements, and -
    in § 268.7(d)(l) to be submitted to the
    EPA Regional hazardous waste
    management division director (or his '
    designated representative) or State ,
    authorized to implement part 268
    requirements.     .        '  .-,

 -  C. Section 268.9          ''    '  '   •  .
     A typesetting error was made in
  .  § 268.9(a). which repeated language that
    already was in the paragraph. The  .
    paragraph is located in the middle
 :   column of 59 FR 48045, starting with. If
   the generator determines that .his waste  .
    displays the characteristic of ignitability
    *,-* * and finishes with; as specified in
   paragraph (b) of this section. -This
  redundant portion of the paragraph is
 .  deleted in today's amendment..  .    "
  Additionally, in section 268.9(d)(2)(i) it
  states that in treating wastes that exhibit
  a characteristic, the underlying
.  hazardous constituents must also be
  treated, and if not, the certification in
  § 268.7(b)(5)(v) applies, there is no
 . section 268.7(b)(5)(v), and instead the
  intent was to-reference the pertifieation
  under section 268.7(b)(5)(iv). The   '.
  erroneous reference is changed in ' •
 'today's amendment..
  D. Section 268.40

    EPA established that for certain
  characteristic wastes managed in non-  '
  Clean Water Act (CWA) wastewater
.. treatment systems, non-CWA-equivalent
  systems, or non-Class I injection wells, •'
  .the underlying hazardous constituents
  reasonably expected to be present in the
  waste at point of generation should be
  treated as well as the hazardous
-  characteristic. For D018-D043,   -V  "
    characteristic wastes, this applies to
    both wastewaters and nonwastewaters
    While in the consolidated treatment" :
    table in § 268.40 it is noted that the-:   '
    D018-D043 nomvastewaters need to
    meet § 26_8.'48 standards, this is not
    indicated'for the wastewaters. The
    corrected table will include the .
    requirements, for wastewaters that are
    managed in non-CVVA wastewater •
   .treatment systems, non-CWA-equivalent
    systems, or non-Class I deep injection
    wells.
     An improvement iri the Phase II final
   rule was the simplification of two
   equivalent technology-specific  ..
   combustion standards in: Table 1— •
  . Technology Codes and Description of   -
   Technology-Based Standards In 40 CFR
   268.42. The Agency consolidated the
   descriptions of INCIN (incineration) and
   FSUBS (fuel substitution), by combining
   them into one term, CMBST,
  . (combustion). In prior rulemakings, the
   treatment standard for both wastewaters
 .  and nonwastewaters of Acetaldehyde
   (U001) was listed as "FSUBS or INCIN-"
   In the Phase II final rule, a
   typographical error left out "FSUBS"
   and only listed the treatment standard,
   'INCIN." The treatment standard for
  .U001  is thus changed from "FSUBS or
  INCIN" to "CMBST."
    The following changes are also made:
    • For Ethyl acetate, under F001, F002
  F003,  FQ04, and FOOS, the CAS number'
  is corrected to read, "141-78-6;" -
-   • For Tetrachlofoethylene under
  K043,  the CAS number is corrected to
  read, "127-18-4;"   j   •   ,  -
.    • For Diphenylamine under K022 and
  K083, the CAS number is corrected  to
  read, "122-39-4;" "•;    - \   .
  . ••  Forbis(2-Chloroisopropyl)ether  "
  under U027, the CAS number is        -
.corrected to read, "39638-32-9."
-   • ForPhthalicanhydride.underK023
 K024, K093, K094, and U190, it is
 clarified that Phlhalic anhydride is'
 measured as "Terephthalic acid," or '*
  Phthalic acid," which are synonymous
 terms for the same substance.    .   ' -
 These changes are all made In the  *•'
 consolidated treatment table in section
 268.40 in today's amendment.      '   • ,
    (incineration) and FSUBS (fueli-    •  .
    substitution) into one term, CMBST '  :
    (combustion) made no substantive • - -  •
    change to the promulgated standards,  :
    aad, therefore, "did not require notice  -
    and.comment: The Agency's leaving out
    part 265, subpart O in the definition of
    CMBST (combustion), therefore, was an
    oversight that.is being-corrected in    • -''
    today's amendment. Furthermore, the
    parenthetical statement on page 48002
    about part 265 interim status standards
    was not intended to be in the preamble, •
    and should be disregarded.   '   -
 '  F. Section 268.48       ' ,  '  '  '     '

     In the table of Universal Treatment   .
   Standards, it was footnoted that zinc   •
   was riot considered an "underlying
   hazardous constituent" in characteristic
   wastes, according to the definition at
   268.2(i). Vanadium also  is not      '
   considered an underlying hazardous   '
   constituent in characteristic wastes, and '
   thus, is appropriately footnoted in this
   table in today's amendment:

   G. Appendix X to Part 268
    As was mentioned in the amendment
   for 268.7(a)(8), EPA modified the
   alternative treatment standards for lab
   packs from identifying the.'wastes that :
   can be included in lab packs to
  specifying .those wastes that are
  prohibited from being placed in lab
  packs. As explained earlier in this rule,
 ,the language of the § 268.7(a)(8)
  certification is being changed in today's ~
  rule.  Appendix X is also being changed
  to include the revised certification
  language for the convenience of the  •
  reader.        '    •••'..'.'  '•

  III. Clarifications   .   /     .    :

 .A.. Clarification of State Authority Policy
 E. Section 268.42
 , • The definition of combustion >
 (CMBST), as stated in § 268.42 Table 1,  •
 is::"combustion in.iricinerators* boilers,
 or industrial furnaces operated in .  ;
 accordance with the applicable  '  •
Tequirements of 40 CFR part 264 subpart
 O, and.part-266, siibpartH." The-
 defmition inadvertently deleted the -'
management of hazardous waste during •
the period of interim status, covered in
part 265, subpart O. At 59 FR 48003,
EPA affirmed that combining INCIN  '
                         .

   The Universal Treatment Standards
 (UTS) were promulgated in the Phase II
 final rule pursuant to HSWA authority.
 In most cases UTS are the same levels
 'as the previous LDR treatment; ;  .
 standards, while about forty'percent of ••
 the levels went up or down.ln most of
 these cases, the change in the limits -     •
 actually reflect adjustments in the limits  •
 of analytical detection, thus actual •'.H
 treatment will likely continue to destroy1
 or remove organics to nondetectable •
 levels. Even in those cases where the   •
 level has changed, the technology basis
 of the treatment standaf'd has not. •' .':  -
 Therefore the changes  to the^ treatment:
 standards should-not be viewed as more
 or less stringent.   ''   •    "   .•.-.-.
  Concern has been raised regarding    -
how Ihe UTS should apply, in States -   ' -'
authorized for the LDRs; specifically,''•  *
what treatment standards must be met   •"

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  244        Federal Register  / Vol.  60,."No. 1  /  Tuesday, January 3, 1995 / -Rules  arid Regulations
  "by a facility located in a LDR-authorized
  State: the Phase II UTS levels, or the  •.  -
  treatment standards in a State's..
  authorized RCRA program? An,
  additional concern is whether the
  authorized States would lose their
  ability to implement their LDR  .  '
  treatment standards if they were
  superseded by the UTS.
    A memorandum from Michael
  Shapiro, Director of the Office of Solid
  Waste, to the EPA Regional Waste
  Management Division Directors,
 •announced that the new UTS are neither
  more nor less stringent than the   "   • •
  p.rovious standards. Therefore, the ne'w
  standards do not supersede existing
  standards in States authorized. States
  authorized for the LDRs for some or all
  \vaste streams would continue to
' implement the treatment standards for
  the streams for which they are
  authorized. The new UTS do not apply,
  for those waste streams, until the State
  has incorporated them into State law.
  EPA strongly urges States to'implement
  the now UTS standards as soon as
  possible, both for simplicity of
  implementation and national    .   •'
1 consistency. In any case, State law (as
  interpreted by the State) would
  determine which standards applied.
 This approach would avoid the dual
 regulatory problem which would occur
  during the time before new HSWA   •
 requirements are adopted and
 authorized in the State.
   EPA has a strong interest in
 uniformity and consistency of
 regulations and believes that the
 improvements'in die UTS meet these
 objectives. Thus, States are encouraged
 to adopt and apply for authorization of
 the Phase II LDR rule. States that are '
 currently authorized for portions of the
 LDRs may submit an abbreviated
 "authorization revision application for
 the UTS. Details about what would be
 required for this abbreviated
 authorization are in the memorandum,
 which dan be obtained by calling the
 RCRA docket.    ,       .    ,  ;.
   It should be noted that the Agency,'
 generally, is not relinquishing its
 statutory responsibility to implement
 significant new HSWA rules in States as
 soon as the rules become effective: The
 new approach set out in the
 memorandum is reserved only for areas
 of the hazardous waste program already
 authorized and regulated by the States,
 not now areas of the HSWA regulations.
 For example, the Phase II rule' ..
 established treatment standards for
' several newly listed wastes; those new
, requirements are immediately effective.;
 in the States and will be',cnforce"d by
           ••         !               -
 B. Flowchart Clarification
   EPA is clarifying in' today's •.'.'";";•
 amendment the.Phase II flowchart;
 entitled, '.'Implementation of Key Phase'
 II LDRs," at 59 FR 48018. The second
 block from the bottom left pbses the '
 question,,"Is the waste a mixture of a
 newly identified TC organic waste   '  .
. (0012-^43) with a prohibited listed  .
 waste.  . ." This language is not correct
 and should read in full: "Is the waste a
 prohibited listed waste, or'one of the
 newly listed Phase II wastes, that also  •
 exhibits an organic toxicity    '
•"characteristic?".   '             ,    "
 .  Another clarification is being 'ihade on
 page 48021, in the first diamond.' •
 Questions have been raised as to
 whether the "constituents" mentioned '
' there include underlying hazardous
 constituents. No, "constituents" does
 not include UHCs. The wording inside
 the diamond should say "Does the
 treatment standard for the listed waste
 include the treatment standard for the   '
 constituent that causes the waste to
 exhibit the characteristic?"

 C. Telephone Number Correction  ..
   . At 59 FR 47983, Richard Kineh's   _•  '
 name appeared as an EPA contact for •
 "other information" about the Phase II
 final rule. The phone number provided
 in the Phase II rule, (703) 308-8414, is
 incorrect; Mr. Kineh's telephone  •  •
 number is (703) 308-8434.
 IV. Rationale for Immediate Effective
 Date      '    ..      .     .  '.
   Today's notice doe's not create any
 new regulatory requirements; rather, it
 restates and clarifies requirements
 already in effect by correcting a number
 of errors in the September 19,1994 final
 rule (59 FR 47982). For these reasons,
 EPA finds that good cause exists under'
 section 3010(b)(3) of RCRA, 42 U.S.C.
 9903(b)(3), to provide for an immediate ,
 effective date. In addition/there already
 was full opportunity to comment on all
 of these issues during the rulemaking so-
, that further comment is unnecessary.
- For the same reasons, EPA finds that
 there is good 'cause under 5 U.S.C.". • •
 553(b)(3) to promulgate today.'s  .   ;.,'.-.
 corrections in final form and that there.
 is good cause under 5 U.S.C. 553(b)(3)
 to waive the requirement that
 regulations be published at least 30 days
before they become effective. Finally,
EPA jibtes that although it is not  '..;. •
•withdrawing any existing regulatory-
 language, all of today's revision's operate
prospectively.'     •    .'..'••'•: ••  ."••••

V.'Executive Order 12866"../ ,      ". ."
 review under the Executive Order. Due.., ':. " "-
 _to the nature of this regulation.,.- •"?-. i'?';••' ,."', ,;
• (technical correction), it is riot.:" j;/^-:.....  '• •..-,.'
 "significant";.therefore,xnbExecutive -!.. •'.',•
 Order 12866 review is.required. •. -,  '"..-<   •  '.''

 List of Subjects in 40 CFR Part  268 ;'.,.. '  :  .-.;'
   Environmental protection, Hazardous'.
 waste, Reporting and recordkeepirig   :, .'
 .requirements.'    •   ".'••!"'.'•    . c
   Dated:'December i6,1994.   ' - .; "•'•" _^ ' '. '-
 Peter Roberts, '   •"'"  . ••      ;.  '.'  ."'   '. • :
 Acting Assistant Administrator for Solid .'• '- •
 Waste and Emergency Response.'.'   '.<'"'  .-''••'  -
 ..  Fortherea'soriKseto'utin.the .  .>.>',.
 preamble,-title 40 chapter I of the Code.
 of Federal Regulations'is amended to  •   .
 read as follows:  •     '.   .    •''••.-.

 PART 268—LAND DISPOSAL     .:.,.
 RESTRICTIONS        -  1      , :

   1. The" authority citation for p'arf 268   ..  .
 continues to read as. follows:..-.-   .      •
   Authority: 42 U.S.C. 6905,6912(a), 6921
 and6924.'  .  '}   .' ":;  .  ; '  •'

 Subpart A—General    .     •         .:;-. "

   2. In § 268.2, paragraph (ij is revised,
 to read as follows:  •  ••   ;  .-•••• '-•;

 §268.2  Definitions applicable In this part.
 .  (i) Underlying hazardous constituent
 means any constituent listed in.
 § 268.48, Table UTS—Universal ','.
 Treatment Standards, except vanadium
 and zinc, which can reasbnably.be  ". •• ..
. expected to be present at the ppint of  :   ,
 generation of the hazardous waste, at a •
 concentration above the constituent- ......
 specific UTS treatment standards.  ',.  •.  ..-
   3. Section 268."7 is amended by  , •
 revising the introductory text of s : ,'   *'
 paragraphs (a)(l) and (d); revising   " •:
 paragraphs (a)(l)(ii); (a)(ll(iv); (a)(l)(v),  . •
 and (d)(l); and by adding paragraphs  .. •
 (a)(l)(vi) and.(a)(3)(vii) to.read as~tf.f.. :^.;. ,
, follows:', f.  • '"•-;'.-..:...:.::.'...'•:•;•••'•".' •;•"?,-.'?''"••!'•< ;' '••.
 § 268.7  Waste analysis and recordkeeplng.' ;  ;

   (Ij If a generator cietermines that he is .  ,
 managing a restricted waste under this, . ..
 part and the waste does riot riieet the "/  ....'•
 applicable treatment standards set forth, •
 hi subpart D of this part or ttexceeds  .
 the applicable prohibitibri. levels set ,•-.. .  ,-.-.
 forth .in §268.32 or RCRA section-}c;>:".    ..'
.3004(d), with each shipment of waste •"•!• -'••
 the generator must notify, the treatment;; .•; -.1 ,,
 or storage facility in writing. The notice!'..'•  .
•must include the following inforrnation: .- .  ."
'•'• Under Executive Order 12866,-EPA;  ... .  (ii)The:waste constituents thatthe ,Vi ::/.-.:.•. .V-
must ju'dge^ whether a regulation is.  <;	 treater will monitor,1 if monitoring wiilci'.'-.vV >,;.•
"significarit" ;and, therefore, subject to .! ' not-include'-all regulated ^6ristituents,;v:..rv «;,•••

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               Federal Register /..Vol.-60, No,  1'/ Tuesday. 'January 3.  1995 7  Rules ahd: Regulations-\
                                                                          245
   for wastes-FOOl-FOOS, F039, D001,    '
   D002. D012-D043 and in §.268.32 of
   RCRA pection 3004(d). Generators must
   also include whether the waste is a
   honwastewater or wastewater (as •
   defined in § 268.2 (d) and (f)), and "   •
   indicate the subcategory of the waste •• -
   (such as "D003 reactive" cyanide"), if
   applicable; -        .   '    , .
 •*,*.*    *   *        •    •
    (iv) For hazardous debris,  the
   contaminants subject to treatment as
   provided by § 268.45(b) and  the  - •
   following statement: "This hazardous
   debris is subject to the alternative
  treatment standards of 40 CFR 268.45;"
    .(v) The waste analysis data, where
  available;  and,  '  f. ' '
    (vi) The date the waste is subject to  '
  the prohibitions.    •
   .(2V*  *  *   "
 .   (0
    (B) The waste constituents that the •• •
  treater will monitor, if monitoring will
 'not include all regulated constituents,
 - for wastes F001-F005, F039,  D001,
 D002, D012-D043 and § 268.32 or RCRA
 section 3004(d). Generators must also
 , include whether the waste is  a
 nonwastewater or wastewater (as  "
 defined in § 268.2 (d) and (f))", and .•
 indicate the subcategory of the waste
. (such as "D003 reactive cyanide"), if
 applicable;       ,        .     •  '  ,
 *  •• *   '  *     *    *
    (3) * *  *         . '   •       -
  ' (vi) For hazardous debris when using
 the treatment standards for the  •
 contaminating waste(s) in § 268.40: the
 requirements described  in paragraphs
. (a)(3) (i), (ii), (iii), (iv), and (vii) of this v
 section; and,     •    .'
    (vii) The date the waste is subject to
 the prohibitions.   •,' '
 *  .  ' *   .  *    *     *       - .
    (8) If a generator is managing .a lab  •
 pack that contains none  of the. wastes.
 specified in 'appendix IV of part 268,
 and wishes to use the alternative
 treatment standard under § 268.42(c),  -
' with each shipment of waste the
 generator must submit a notice to the
 treatment facility in accordance with  .
 paragraph (a)(l) of this section, except  "
 that underlying hazardous .constituents
 need not be determined.' The generator
  must also comply with the requirements
 an paragraphs (a)(5) and (a)(6) of this
 , section and must submit the following '
  certification, which must be sighed by
  an authorized representative:  .'.-'•'
    I c'ertify under penalty of law that I
  personally have examined and am familiar :
  with the waste and that the lab pack does not
  contain any wastes identified at Appendix IV
  to part 268..I am aware that there are
  significant penalties f'pr submitting a false
  certification including possibility of fine pr
  imprisonment.'     j:~        ,
 .*'•'*'..*•'•*' '' ". *'
    (b)'*. *>.      '       .' .".'"•      '  .
   -(4)* * *   .       .      '        :.
    (ii) The waste constituents to be   *
 monitored, if monitoring will not
 include all regulated constituents, for   .
 wastes F001-F005, F039, D001, D002,
 D012-D043 and in § 268.32 pr RCRA
 sectibn-3.004(d).; Generators must also
 include whether the waste is a
 non waste water or wastewatef (as
 defined in § 268.2 (d) and (f), and
 indicate the subcategory of the waste .
 •(such as D003'reactive cyanide), if  '
 applicable.      '.','•   ,  .
 *    * •   * .    *. ! '*
    (d) Generators or treaters who first
 claim that hazardous debris is excluded
 from the definition of hazardous waste
. under § 261.3(e)  of this chapter (i.e.,
 debris treated by an extraction  or
 destruction technology provided by
 Table 1, § 268.45, arid debris that the'
 EPA  Regional Administrator (or his  . -
 designated representative) or State
 authorized to implement part 268
 requirements has determined does not
 contain hazardous waste) are subject to
 the following notification and  ..
 certification requirements:
   (1) A one-time notification, including
 the following inforrnatiori, must be •
 submitted to the EPA Regional   .
 hazardous waste  management division1
 director (or his designated
 representative) or State authorized to ..
 implement^part 268 requirements, or
 State authorized to implement part 268
 requirements:  '    t
 *     *"•*,,*'*
  4. Section 268.9 is amended by ".
 revising paragraph (a) and paragraph -
 (d)(2)(i).to read as follows:    '
   §268.9  Special rules regarding wastes that
   exhibit a characteristic. •,',..•';
   .  (a) The initial generator of a solid  :
   waste must'determine each EPA '•:•'•.'  -
   Hazardous Waste Number (waste code)
   applicable to the waste in^order to'
   determine the applicable treatment
   standards under subpart D of this part.'
   For purposes of part 268, the waste will
   carry the waste code for any applicable
   listing under 40 CFR 261, subpart D.' In
   addition, the waste will carry one or
   more of the waste codes under 40 CFR
 .  261, subpart C, where the waste exhibits
   a characteristic, except in the case when
   the treatment standard lor the waste .   '
 •  listed in part 261, ;subpart D operates in •
   lieu of the treatment standard for the  •'.'
  waste under part 261, subpart C, as',
  specified in paragraph (b) of this- .      V
  section. If the generator determines that
  hte waste displays the characteristic of-  '
  ignitability (D001) (and is not in the  '
  High TQC Ignitable Liquids Subcategory
  or is not treated by CMBST, or RORGS),
  or the characteristic of corrosivity
  (D002), and is prohibited under  ••
  §268.3 7; or that his waste displays the .  "
  characteristic of toxicity (D012-D043),
  and is prohibited under § 268.38, the
  generator must determine" the  ;.'•'•
  underlying hazardous constituents (as
 •defined in § 268.2), in the D001, D002,
  or D012-D043 wastes.'   '  j.  '.     '    .
  *    *     *    *••'•* •''•' -.  •   '   .- •
   (d) *.  * * .    "•'   '.'/'  •    ' •    . '
 ."'(2) *•.'•'*   -;     ;.    .,:      •'
   (i) If treatment removes the   .-      -.
 characteristic but does not treat   ,•"*
 underlying hazardous constituents, then  .
 the certification found in:     '     '
 .§268.7(b)(5)(iv) applies.  -"   ..: .,     '
 *•••*••-.'*•   *   • *    	   ;  . s•
.•'•--'.     •     *  •*'.'•*•

 SubpartD—Treatment Standards   .  ...

   5. Section 268.40 is amended by
"revising the table "TreatmentStandards
' for Hazardous Wastes" to read as.,-
 follows:  :- •_...''••.-''    .  " .•;"."   •

.; §258.40   Applicability of Treatment
 Stcindards.   „..   •   ;-...•
 '*-•  ••*'  '*; '.••*'*.••   •,- •  ..  '   .
' BILLING CODE 6S60-50-P .  '

-------
246   •    Federal Register / Vol. 60. No. 1 / Tuesday. January .3, 1995 '/ Rules and  Regulations
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wMrt'cya'rildes are uiidlh ilia process. •. '. . ..•"•"
'•'•"-. ':. '! "r ' ' . ,.'•"/.'-•', "••'•' '•;•;. •'. ', '',"'•'. ..:>•'
diMnch^t.bith r«j'k»uM.(r()M;(jij Mt.hs (rorji rfo'fil rUaf Mating 6peratl6nt
: •.-•-• ..'is.-'. ,'..'..•.-...'',.>• .,,-?.''..'.'• ••:••' - \-'.' '•'• "
Sttnt. eyatatt wWtieM Trorri aatt bath jWt dewirij from metal httt treating
"•;.;'•• :•;.: '.''•: :-•.'.•"'. ,':; •,•.•'':';•.''•"••'.;';.>'']'." •'
;•...•.'./;.,.>" •- '• v. .•;•': - .,••':.':.•.:.-.!..:..•.!,. .'•. ,v. ,-. •. :;:-..iJ..- ,'.. ... . • . ... -
vi;^S^^^^J.^V.f;;^;^r"
^•.:;..;;;.::;..;r,-,i<% .-.•;*,•,. :=:.X'-'.: •-'.'''., •- '
i!^'^^'-'/'^"'.''.^^.'"''" "• -•'':::/i •"•'",•• .
/.V,' .,!,: .;V. -;..••.;••...'..••,. --p:- „;.-.. ..'.,•:-•:•: ,-:-, .'
'*SSSS^.w.^ • '•
when such (tiosphatlns j» «>» i exclusive conversion ebatina'piocess.
••>-^.>:«: -,-,.;•.; .-:>-.,..•>.:, ..;-,.-•;...;./,,.. ,•.,-•;.•.
.- .;; ;;• ftEGULATEb HAZARDOUS CONSTTTUSNT' . '
:;;3:ycfe^r;;:,,.
ihWit. -,:•':'-:'• /; •'.-••. ' - " :
ini^-t--Yr.--''':f-;.'-- ,- ••'/.
.tA**** -.; :.,',;>!s.-. •*"•"•

.Cvsnldis (Total)1. ;,..'..•'•.. ' /'.

••Uid-;.,- .;.."., ,.;,.•; .. '. • . ' .
fteliil'"'-1', •''.-. .'• " '• -. -. "•. ... •
.'Sinie'r "':- ..f',.'. '""•"< • • "...- ••' . .' ' ' •

.'CaSfn'l'um •",.. !," -„•: '-'••' • • ..
. Chromium'iTotaH .;.;':.,',.., .- .. '..-.. .!
.cyjnte'rtot^ .:.;.;',., \ ;.; .: -

jtwd ;'-.^..v..,'t :ri, :-...; •.•,-•,.•
.flickel- .•-;• ;;.; / ' .' - . : ' .'
•iiwr'X'lv '.«•. ?'-•>' . .v .
l-iriMAot*^'.-:.'-..-,-:1 •.,;:•,, .

•'c^d*J'(/«al)* v •••;•• /.; v-- ,

1«kl"-<..-; ••>/'-.,-':'• '••• . '.'•'. • '


Crirornhjni (Total) • . '•'' " . • .'
sCyilnWi>i'(Totalir- ' " .' '•. . , ' . '
'cya nw« (ArtSMble)'!,. , . - • . '
: ^^
-74400Z-6
•744b:2i.4'
'."•'7446U3-9 ''
"7440-47-3- .
57-12-6-
'. 57-12-5
7439-92-1 .
. 'MAOfe-O
W^i.224-:
. 57.12.6 ••>••

' '. 7.443-47-3 '. ,
57^12:5.. ' :
•. 5.^t2-S' •'
' >«9-92-i '•
., 7440^2-0 .
: -74'40.22'4.
'.. 7446^3'-9 '
••.•M&14 ...
•.;•'.' BWJ-S • .
.'.sWi-s,..';'
'• 7«94i-1
'7440-62-0 •'"'!
.744*22-4
744647^ '•-'•
. 67-12-5 '•
' :67-12-S" '
WASTEWATERS . ..
Concehtra'tion In mgfl1;
or Technology Coda4
. • • -' -3.98 • •' : .
; ' ' , •••-•• NA - '- • '••"
• ; NA"- -: . v ;. •
.-'. '• - . 2.77
•• 1.2 ;" '•
. . .6.86 "
• , . .'6.69. ' . .' . •
.,-"•• • 3\98' ' , -
• • '•' '•' • M • •
.•.\.,:.V:-^ ••• .

•'.. ..-.-" • i.ii •
1:2
-•- . - ' 0.86
-1 -. ... 0.69 • . .
' '. • , v '3.98. .- '
-1 ••• - ':-:«A-' ' '•-' '
' ' ''.:•' ', NA"."'
., /V '.-,:•'. "2V77 ". ' '
''.\ '.' • - '.1.2 • '•'"• •
.-.-.. . 0.88 ..
. ' 0'.«9 '-" '. • '
• .' ' '. 3.98 '-" .'.' ':~.
'NA - .
" - "• ' :'2.t7 ' ' •
-.'•'-• - 1.2- :
, •.• '-..:.o.86- "".'• :-

. NONWASTEWATERS
Concentration in mg/kg*
• unless noted as.'mg/l TCLPV
,5.0 mg/ITClP
. - '6.30 m'g/ITClP ' . >'
. 0.19 hlg/ITCt.P


30 ' . :

' -5.0 mg/lTCLP .
0.30-mg/ITClP
. 596- ' ' ."'


: .-'-- -.690
30

"... 5.0 mg'/ITCLp'




;.' • -36 •"• •';.-'


• 0.30 nigflTCtP' ' ' .
... 6.86 nig'/ltC!/ - ' '•-
"' ''-• S90- - •<''"•'••
'••-•••'''"•.ao'-'T".--.""-

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-------
254      Federal Register  / Vol. GQ~, No.  1  / Tuesday,'January 3,/1995 /  Rules and Regulations
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-------
                                                                    TREATMENT STANDARDS FI?R HMAHOOUS WASTtS     -
                        Waste Description aridTrearoeht/fleftuloiory SuWateasry
                                                                                                                                               unless noted as -mj/l TCU";
                                                                                                                                                  efTeehnolor)yCodf.
                                                                     2.3,4.6,-TetraerilQrophenot

                                                                     P«niadHerophenol

                                                                     An F024 wastes
                                                                    HexacNor'oe'thane  .

                                                                    Chromium (Tom)

                                                                    Nlciel _'


                                                                    Carbon lettaehtorlde
                                     rvlnn™,!^*^'°"0tterantfn|'''Cm     et"°«"«
                                     nrtng afliounts-ana.positions of chlorine ,..
                F026 • Uolit Ends Sufx^tejory
                                                                   LUMchforoeitiylene '.

                                                                   Metilyltne eMorldt

                                                                   .|.1.,a-Ttlchloroetrune
                Krtsri tWn torathi *W«IM fwi w to wd i«w^, o-T^ ^^8
                ^oOT,»8m,pos,tio^.0(^Mw^™i^1«lu«»«.?«
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-------
                                                                                      \
 256     .Federal Register / Vol. 60,, No.-1 //Tuesday,.January.3. 1995 /.Rules and,Regulations-,
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-------
                                                                                     TREATMENT STANDARDS FOR HAZARDOUS WASTES •
Waste Code
  -F038-.-
 F039
                .'. ::  ...WastoDescriptionand. Treatment/Regulatory Subcategory1
               Petroleum refinery-secondary (emulsified) oilfwaterftolids separation- slutfaa •
               aooyor float generated from the physical and/of chemical separation of    '
               •bilrWarer/solids In process wastewaters and oily cooling wastewaiers from
               petroleum'efintrles. Such wastes Include, but an not limited to, all sludges
              •tndfloats-o«rwat«dlnrlnducedilrfloatatlon-tiAF)unlls,tanksand	
               Impoimdmtnts, and all jludan owwatod In DAP wills.  Sludgw c«narat«d
               In itormwaitr units that do not rectiva dry weathar'flowr«lud8M ganeratad
               from non-tontaet oncMhrouah cooling waters sagragaMd for traaiment
               from othaf proctss or cfly cooling wata«; sludgn and floats gtnirattd In
               »gor.5jlvt bkHogleal matnwnt urtta at daflnad In 1261.31(b)(2l (Including
               aludgaa tnd lloits genefitad in on> or mor« additional units aftar
               wastawatara havt bean treated In aflgresslva biological units) tnd F037
               K048, and KOS1 are notlnduded In this listing.
              .tachat* (llqulda that hrva percolated through land disposed w«5t«j)
              ttuWng from ttw dfsposal of mori than one restricted waste classlllM M
              nardout unoat tubpart.p of this part.. tttKhaie rasuHIng from th»  '
              T«ofon.«mo"

                                                                                                REGULATED HAZARDOUS CONSTITUENT
                                                                                                                                                           Concantratlon in
                                                                                                                                                            or Technology Cods4
                                                                                                            Concentration in mg/Vo.'
                                                                                                          unless noted as 'mg/1 TCI.P*;
                                                                                                              or Technology Coda
. bislZ-Ethylhexyl) phtfialate  ""
                                                                                      Naphthalene
                                                                                      ^•MBMMM

                                                                                      Flwnanthrene
                                                                                     Xy.lan'es-mlxad Isomers        •   !  .  -
                                                                                     !5umafo-,rn-. mi p-syisno concenirsiiofisi
                                                                                     Chromium (Total)

                                                                                     Cyanides ITbtW' .
Acariaphthant'  '""
                                                                                    2-Acatylamfn'6lluoren«'••''-  • -"'•
                                                                                    AcrylanltrUa'
                                                                                     •iu.i
                                                                                     ildrln'.

                                                                                    «-Amlnoblphenyt
                                                                                       .^
                                                                                     rillc'rie '.'.• '• '..'.'

-------
258	Federal Register / Vol. 6Q,':No. l'./ Tuesday. January 3, 199.5 •/Rules and .'Regulations •
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                                                                   TREATMENT'STANDAROS FOR HAZARDOUS WASTES
Wasw C0d«
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  •• ' • Waste Description aftd Treatfoent/ReQulatory Subcategofy*



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..'•,..' •' . •-•: -' •'• •'. . .... v. ....
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Ethylsne dibroiiilijs (i,2-6ibrorto«lhan«) ; '

i.^DW.iijlfhteipn.-noxyac.tie.ckn"". ' '

p^Dji-, •,-:;• n;- :.. .-...,, ,v

Mf^M :•••„•-.-.• ,.-,,. ..,:•..•-, ,
».<^r,..';-. ••>:,,,:>/ •..:.:,-,. .

D^Mmttti"--.., -:„•,•;-.: •


CAS'NuMber
111-91 r
111-44-4 .
-. 67-66-3 '
39638 32-9
59-50-7
74-^7 3
•91-58-7 "
9S-57-8'
167^5;i '
218-61-9
95-48-7 ''
108.39-4
;t6'6-44-S
• 168-94-1
' .98-12-8 ; .
•106J9J-4-- •
^'74:953 • •
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WASTEWATERS ".
: ' Concentration in mg/1'; .,
'•' ' of Technology Coda' v

• • . 6.033 '






6.036

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- '.- . -0 77 -.

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:_:;- '.'; 6.636 ;;...;. .


Concentration in tog/kg* • '
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200       Federal Register ./ 'Vol. .00. "No. 1 / Tuesday, .-January 3, 1995 / Rules .atfd iRegulatioris


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-------
- ,  TREATMENT STANDARDS FOB HAZARDOUS WASTES


Wasn Cods'













..;. -.:. •.
• K071 . •


,K073 ;•-'
	 •••;•-, - •
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" • ' t . - . > \
Wasta Description and Treatment/Regulatory Subcategory'
','"•" .'."'''•" "•• . ' • •

..: ."--.-• ' ..•••••.
' - '• ".»..• ' ' •

•.-.-.".. - '' ' • '•


Spent pickle liquor flenerated by steel finishing operations .of facilities within
•the Iron and steel Indu.try (SIC Codu 33 Land 33S).


Emission control dust/sludge from secondary lead smelting. . Ceiclum
Sullate (Low Lead) Subcategory . ' .

emission contra ausmiuage rrom tecontf|ry lead smelting. " Non-Calcium
Sulfate (High Lead) Subcategory ......
K071 (8rin« purification muds from the mercury cell process In chlorine •
production, where separately prepurlflod brine Is not used) nonwastewaters
that are residues from HMERC. ..'..." . '
K071 (Brine purification muds from the mereury.ceO procesi'ln chlorine
production, whero separately prepurlfled brlna Is not used.) rwnwastewatsrs
that are not residues from RMERC, . .
Alt K071 wastewaters. ... •>
Chlorinated hydrocarbon waste from the purification ttep of the diaphragm
sril prsSsss tains B'-ipSt. iftStfoi in chlorine production.
- c'..- - " •••."••'•'••. . " ' " .
.••-•' •;' •'. :•.'•'-... .••..: •" ~. . . -. • '.-•
' • . ' • . "• •,.'.•'-< '' •'"'..' '
Distillation bottoms from anllftu production;.. ' -V . ••.'•••

•-....-...,(•.- '-' .-'• .-'. .;••-•.;• . ', •. '/..• - .. ... .
. • '." ,y ,• Y 't . • ;......;... . , - : , '

REGULATED HAZARDOUS CONST
• . . Common Name
.Chromium '(Total! . ' • '
Lead , ....
Mercury ' • - ;•
.Nickel '•
Selenium ... ' , .. ....
•Silver , •
Thallium ' .
Zinc • • .
Chromium (Total) • -•'. .. - ..^
L.id '•...'
Nickel :' . . < ' .
Cadmium ' 	 '....'
lead . . • . ..
sf -'-".""•"."
Mercury - • ' • . ' . -
•••' ' ' '"!
^Mercury
Mercury - •
Carbon tetrachiorlde
Chloroform
Hexachloroathane'
Tetrachloroathylena ' '
•Aniline ' • • •, '..•/'• • . .". .'
Benzene . ' ' .. ..' ,.
Cyclohexanone '.' " ":""."-'."•: '-•" '


TUENT
CAS' Number
. 7440-473
7439-92-1
•7439-976
7440-02-0
7782-49-2
7440-22-4
NA

• 7440-47-3
'7439-92-1

•-. 7440-43-9 •

NA
7439-97-6
••7439-97-6
7439-97-6
56-23.5 ^ '
' 67-66-3 .
67-72-1
127-18-4
62-53:3 .
71-43-2
108-94-1 '


WASTEWATERS
• Concentration In mg/1'; . . .
or Technology Code*
777 •" ' • • '-•
0.69 .'
NA
• 3.98 • '
NA • .
NA
NA ' •.

2.77
0.89 ••

. ' ' '0.-69-

. . ." NA ...
• •' ' NA' ••. ' ' '.'
• ' ' . ; NA '. ' • : -.
'o!is ' ' •
' '. O.OS7
0.048 . .
' 0.055
, 0.056 - ••• .
0.054 '
' ' .0.81 .-"--"•
' 0.14 :' - ' • •


.
NONWASTEWATERS
Concentration In mg/kg»
" ' unless noted as "rag/I TCIPV • ~- •










' •'•- "NA •


RLEAO'' .' .
' "0.20 nigflTCLp' " ""••
• 0.026 mg/1 TCtP '.=,.-- •'•' '
	 	 NA . •- "•'•' •


' ~ ' '-30 •"'•'•• "'.
:- • '. ' :.-.' .'e.o" •-' '' . ';
. . • • . ' .6.0 ..---•
' '.' • •'• -14 . '..' . '.'
• •'••"• . i6-'-,'-- • •• ••


                 -51

-------
UKATMtllT ETAWOAWB FOB KAZAMXWS WASItS
\YJIU c«*s«

K084
K085 •
'. '"' .
:• ••
K088
- /
V/jin Dnoipwo in* Ttt«m*r>un<9tMMy SUxaM^ot'
"'
Wasttwaftr irtllmtnt ttudgti gtntratad during th» production ol vaterlnary
phaimactutlcali from «»nlc or wgano-anenfc compounds.
Distillation or rractlonation column bottoms from the production ol.
Chiorobtnzenes'. - •

"•• • ' - ! • "
• \ !. *
Sotvinl wattes *nd sludges, caustic wnhit and sludges, or wittr washes
,and sludges (ran doming tubs and wjulpment used In the formulnlon ot Ink .
from plgmtnts, driers, soaps, and stabltteeu containing chromium end lead. '
i^--."--^'-.'":;-.---- '-•''', '-•;
•' • '. • •.".-.••• *• . ,• ' . '-
; ' . ' '.
• .-•.' .••'•;•.••••,•.. .-.--...'.-••- '.- : ' •
RTGUWHO tUOMOQVS tOJBTtllXHI-
Cwnmenldmi
D-pimiylimint Wiliest to tft^ngubli liaa
tfpntnvlniiroMmlAe)
D>pr»nylnllr«amln< |<£lncult to drtlmguilti
bixn diphcnylamliw)
Nitiob«nzene
Pritnol..
NIcM • , . ..
Arsenic
Benitne
Chlorobenzent
~ m-Dlchlorobcn;cne
. o-Dlchlorobeniens
p*D!chlorobenzene
Hexachlorobenzene
.Total PCBs
(turn ol all PCS Isomers, or all Aroclors)
Ptntachlorobtmene ' *
. 1,2,4,E-Tetrachlorobenz«ne
. 1,2,4-Trlchlorobenzene
Acetont
Acetophtnone" , ,
,.bte(2-Etr)vlhexyll phthalato , '' --. •'
n-Butyl alcohol • "
. Butylbenzyl phthalate " ••
Cyclohexanone
o-DlcMorobenteno
.Blsthyl phthalata
Dimethyl ptnnalata •• • •.
Ol-n-butyl phthalate -i-

CAS'HinvtMl
m-33A
86-30 S
98-95-3
103-95.2
7440OZ.O
7X4038.2
-.71-43-2 .".
• 108-90-7
. 64173-U
.. 95-50-1 .
108-46-7
118-74-1
. 1336-36.3 .
608-93.6
.95-94.3
, 120-82-1
67-64-1
. .. 96-86-2 .
...117-81-7
. 71-38-3
.85-68-7 ,
. .108-94,1.- v
-. - 96-60.1 - . .
., ...SW6?2 '....
-". .13W.1;3 ....
84-74-2

V/AST£V/ATtRS
Conoointloo in mo.V;
ecTechflotosrCod*'
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092
0.068
0.033
, ' - 3.98
' 1.4 '•
0.14
0057"
	 0.038
.- '. .0.088 .
. . ' 0.090
0.055
... - , -.'0.10
- 0.05S
.-..'.. O.OS5~
. • -0.065-
0.28
• . , . ." 0.010
- 	 -.. 0.28
6.6 .
- • • 0.017
... 0.36' - .
	 0.088
.. . . . .. . 0.20 " ' •
. , •.,. ..-. 0.047
, 0.057


ConctnoittoiinrrvjAo1
wte» noMd w'mfttTCt?*. .-<<


13

62 .

6.0 moflTCLP
., _. -10 ••. •* 	
-• •6.0-— • •" ••• •••
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               52


-------
^ .':....  Federal Register /.Vol. 60, No; "1 / Tuesday,'January 3, 1JKJ5 V/Rules and Keguiatioifc? ;,'
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-------
Federal Register
Tuesday. January 3. 4995 / Rules-and Regulations^ ,.:. -.279

-------
IRfA1UUII. ST AJiOXROS f Ofl IIMAflOOUS WASUS
•
Watt Coda



•
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-'!.'••: '•• .'."'" • . - ' ' •
. K106twastewa'tertreatmenlsludgefrorrithamercurycellprocessin
chlorine production) nonwastewaters that contain greater than or eo.ua! to
260 mg/kg total mercury' ,' .• •
K106 (wastewater treatment sludge from 'the mercury cell process In
chlorine production) nonwastewaters that contain less than 260 mg/kg total
••mercury that are residues from RMERC.. '• ' ""' .
• Other K106 honwas'tewaters that contain less than 260 rng/kg total
"mercury and are not resldues'trom RMERC •
All K106 wastewaters • - , ' • '..-' •• ' •
-Column bottoms from product separation from the production off 1 "
dlmethylhydrazlne (UDMH) from carboxyllc add hydratldes.
- Condensed column overheads from product separation and condensed '
' reictorVont gases from the production of ,1;1-dimethylhydra2lne (UDMH) '
•fromcarboxyliifacldhydraildgs. •• .."• ' '•-
"Spent filler cartridges from product purification from the production of 1 1 "
•'dlmethylhydratlna (UOMHHrom carboxyllc add hydrazldes.
Condensed cdumn-oveiheeds from Intermediate separation from the
production of 1,ti9m.ethylhydrazlm (UDMH) from carboxyllc add
hydrezfdes. . =•- ••• - :r.-—\:- *...:.: v
"• Product viashwatera' frorh the production of dlnltrotoluena via nitration of ,

Reaction by-product water from the drying column In the production of
' toluene'rHarhlne via hydrogenatlon of dlnltrotoluene. • ^ •
Condensed liquid nght ends from_tha purification of toluenediamina In the"
.'•production of toruenedlamlnevIa'hyoYogenatlonotdlriltrotoluene. ...'
..VldnilsHrom the puHflcatloii of'lohienediamlne In the production of •• • . •
toluenedlamlne via hydrogenatlon of 'dinltrotoiune.' ' . •'.'•
.Heavy ends from the piiiilicitlon of tolueneolamlna In the production of
.• . . , ™? ™ . uotoi ene -.-,'•.'..•.-"
• " ACCWAKO KUAROOUS CCVSTrl
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Common ll*ne
CMorooenriN-e
2 Chlorophtnol
c-Dichlorobeniena • '
p-DlcMoroberuana
Phenol • ... •'
2.4.5'Trlchlorophenol
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Mercury ' v .....
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•NA • ••-.,;. . ' -•-•.- . '.-'.'•::,-•"•;_. '
^^-••;:^.; ,..::.;•;>:• .-;.v.;c:;.
Nickel ' . .-'-.""• ^ ' --' i- "•.-•"'• •;

utwr
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" 108907
95578
95-50-1
•106-46.7 •
• 108-95-2 '
95-95-4 \
. 88-062 •
.-.*439-97.6 •
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7439.97:6 •
•;• NA;: •.
"NA% ,
,NA
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' 121-i 2
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-------
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TKMIKOT STAWOATOS roniuzMwous WASTES
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* " Witt* Onoipixxi uv) liwwvtnURt^/jIwr Sufccjujorr1
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gn wv) hytfocNwle idd recovery p>K«>ts a j*od»!«d with iho
pnxluctKXi or alpha. |M methyl I cNortruted tofotflei. ilofl-chlorfMUd
tofatrwi, bcruoyl chlwkJti. «v5 compoundt mth mlMixn o! Ihtio
luncuanil B'oupt
• ... . _..•'.
- / • ..' '.
'•'•'. - '"''. • :•.-"-..- -
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° „ .••• "* .
i , ' "

• VY«ifrw*ter traatment sludgas, exclucfing nsutralfraiion and blotoglcal
.sludges. Qeneraied during the treatment of waslevvaters from the production -
of alpha*u(or mothyl*)'chlorlnated tofuanes, rlng-chtorlnated toluenes, benzoyl
chlofldes. and compounds >vtth mixtures of those functional groups .

.V. .'•...' • ." • *

'" '• :-'.'.• • • ' ' '
«•.'•".•' . . • " • • ..' - •
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1-AcBtyI-2-thloiirea , "' •'••~' ..-'
Acfolkn . • "••:-.'
'Aldtln "..''•-.•• . .-„.-.;'•!.,..•.'...'..•., 	
At'lyi alcohof ' - . '.-• .>/•' .,' • "'.-.' •"
Aluminum phospWda ' .' ' ''. '•'•'* '• "'''-••'• ; | '
• 5-AminomBlhyl 3-isoxa;oIol . '.-..": .''" .•••' '-.'•. ,-.'

tiniirwpvnilini - ••; . ; :. - . - ~ '•'. •'' -
raouAito iw7AWHM« cwtsiir
• Common lljmj
Cjibon teiucNoiKfi -
CWoioloim
.ChloiomelhanQ
p-DICNOfotHIUOM -
H«ic]ch(orob«nieno
'ptntacNoiotunigni
1,2,4.5 Titrichloiobcntirio
1 1,2,2-T«uachl<»oothini
T^uechtp'roQthylQno
1.2.4:TrlcMo«obtnHM •
Beme.rw ' , •
Caibon tetrachlorlde
Cfilorolorm ' .
He^aclilorobQfuene
Pentachlorobeiuena
1r2.4.,5 Tetrechlprpbenzene
Tolrjchloiopltiylens
Tqluep. ' .- ' l
Wfrtarto ' . - •
1:A«tyl:2rthIouf;a
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Aluminum pbosphlda . • ' .
9-AmlnoniQihyl 3-isoxaroto) ' - •
* , .
4-Aminopyndina ' ' .
UCMT
CAS'Ntxntw
56535
67663
74-87 3
1pB'-46 7
11B741
50833-5
95-94-3
79 34-5
1*718-4 '
-12Qf2.1
'71-43-2
56-23-5
67:66-3
118-74-1
608-gq-s
• 9Sr94-3
127:18-4
108-88-3
' 81-81-2 '
691-08-2
107.-pe-8
3.09-00-2 .
10718-6
208S9-73-8
• ' 276^-96.4

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• VMSUWA1CAS
Ccncentiilienin mft1*.
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019
0030
0.055
0.055
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'0.057
p.056
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0.14 ' • .
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. 0.046
0.055
.0.055
0.055 " '••'
0.066 ' '
0.080
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- INCIN
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-------
Federal Register / Vol. 60r No  1 /
.           ..      , p |,.,   • •     •

-------
286   ,»  Federal Register / Vol. 60, No. 1  /  Tuesday, January.;3. 1995 / Rules^and RegQlatibns
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-------
TREATMENfSTANOARDS FOR HAZARDOUS WASTES

Waste Code _

P054
P056 •
PQ57.
• '• --.-'-- L-. .
. P058..
W>59
P060:
.fOB2
	 ro.?jL...._
.P064
. ..P065 .

••. "".
.. ..
.". 	 ; :•„„...-.. 	
''"••"
•••.was1 •
'• ' po67 ~ •"•
P068 . •"
"• 'P069 ' : I"


Waste Description and Treatment/Regulatory SuDcategory'
- . •-, .•*-..•-,..-. '!!-„•
Aziridme ' .
Fluorine '.,."'' ' '
Ruprc-acetamide . ' .
• Ftuoroacetlc acid, sodium s~alt • .
" ' - . •_ ^ . • / ~ 	 	 • •
.Heptachlor ..'"•. . • • " .....'..
' V *
Isodrln • , ' . "., -'•''.'
Hydrogen cyanide ;> '.'•'•'
Uocyanic add, ethyl ester
P065 (mercury fulminate) nonwastewaters, regardless of their t6ta) mercury "
content, that ere not Incinerator residues or are not residues from RMERC
P065 (mercury fulminate) nonwastewaters that are either Incinerator
residues or are residues from RMERC; and contain greater than or equal to
260 mg/kg total mercury.
POtSS (mircury fulminate) nonwattewatert that are ratlduea from RMERC
arid contain lesathan-260 mg/kg total mercury. .'•.'. ' '-
P06S (mercury fulminate) -nonwastewatera that are Incinerator reslduts" and
contain less, than 260 mg/kg total mercury. . \' •
Mettiom»i-_ ;..': • ••••;• • • -..-•;•'•••
2:MBthy|.azWdine / ..,.'••• v ..-•... .-,- • . ' ,' "
Methyl hydrazlno ,.'. ..'••; •• - .-•
Z-TMethyllactonltrile- • • . • ' .'..•' .- '.
' ." • '- .•''•'•,-• ' . - , . • ' •
REGULATED HAZARDOUS CONSTI
Common Namo *
Endrin aldehyde
Atlridine '.
Fluoride (measured In waslewaters only)
Fluoroacetamide
,Fluoroacetlc acid, sodium salt
Heptachlor - • ' •• .
Isodrln .
'Cyanides (Totall1
Isocyantc acid, ethyl ester
Mer
. «cu,y . ^
Mercury ' ' '

Mercury • • --
Mercury • .
Mdhomyl '
2:Met'hyl-ailridirie
Methyl hydrailne • i • •
2-Melhyllaclonitiila

TUENT
. CAS' Number
7421-93-4
l51-:56-4
16964-48-8
640-19-7
. ...62-74-8 .
76-44-8
465-73-6
757-S8-4
57-12.5
624-83-9 • :

7439-97:6
7339-97-6

7439.97-6
7439-97-6
' 7439-97-6
.16752.77-5.
-75-55-8-
60-34-4 ,
. 75-86-5

, WASTEWATERS .
Concentration in mg/l1,
1 • • -or Technology-Code*
0.025
(WETOX or CHO^O) Jb CARBN; or
. . INCIN
•.'/-" 35 •
(WETOX or CHOXDI Ib CARBN: or
INCIN
(WETOX at CHDXD) Ifa CARBN; or
INCIN
0.0012
0.016
' . • . D.921.
• • CARBN; or INCIN
." - . . .- .1.2
'. .' 	 0.86
(WETOX or CHOXO) fb CARBN; or
- - - - - iNCIN -- -•'— 	

NA :
NA

NA
- ... NA . ' .'•
. 0.15
. (WETOX or CHOXDI fb CARBN; or
:. .- • ' INCIN. • .
(WETOX or CHOXD) tb CARBN; or
• . . INCIN ., • .
CHOXD; CHRED; CARBN; BIODG; or
INCIN
(WETOX or CHOXD) fb CARBN; or .
- • • INCIN '- •' -

• NONWASTEWATERS
Concentration in mg/fco*
unless noted as.'m.g/l JCLPr. ; .
or Technolocjy Code

INCIN' •'-
ADGAS fbNEUTR-: ' - -
INCIN' ,.
INCIN ..•-<•/..;."•, .-.-'

- -0,066- .- 	 '. ..
0.066. • . '
•' CMBST
... . ,30 	 ' 	
INCIN .::.-.-., '... .

IMERC: -. . ;
RMERC-

- 0.20" mg/l TCLP.
. 0.02'S mgflTCLP. ';i - -.
NA
• - . .INCIN' ',. •,..'.../•..'.
INCIN ••- -•
CHOXD; CHRED; or CMBST .t ' . ..
' : '- .INCIN '-.'•/• ";..', "'.''.

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                                                                                              I'.',
           '  63

-------
IJKAHtprr STAWMOS f OH HAZARDOUS WASTCS


WtttiCcxfe
FOJO-
ro7i - ,
••"P072-;
- P0731 .
. P07«
— '-•--.

P075. .
• P&76 • '
P077S
1 P078.V
".' P081 ' .
P082'
	 ppa«...-_

. • P085 .
..6087'-. ".
POB8 -
. Lt '-' :•"•
P089..
P092-.'.
'./ ;-'^\f-'-
"".>£*.'.'
.- •.._ ^.. ,
...;. -\fr-~ -
, .."... •• :
•« • > i ••
V/«ttDtKiwkyi*v)TrtJtm«>imts• • '•'"•/ " : " .'
Osmium tanoxlda - - . . '. ' \ ' ' 's
Endbihall . . •; i .. • _ , .
• Parsthlon .-. . . - •.-'•' ' • ,; . _ . ' • ,
. P092 (ptienyt mercuric testate) nonwastewrateni regerdlau ql their total
'mareury content, that aro not Inclnoratw residues or tie not ruldins from "
.RMER'C.' ... .. -..'"•-••••-.:'•. ' ••• '..'••'
.P092 .(phenyl mercuric .acetate) nonwastewatgrs jthat t'ro either Indneralor"
ruldues of ^re tesidues from RMERC; and still contain graater than' or equal '
'. to 260 .mg/kg. total mercury -•.--.-...'-.•.;'-' -•-• ..— -»..•> ,-c,- .... •.
P092 (phenyl mercuric acetate) nonwastewaters'tlut arsjaslduss from • ' '
.RMERC'and contain less than 260 mg/kg total mercury - • . . .
.P092; (phenyl mercuric acetate) honwastewateu that are Incinerator -. , '
resHiKs»nd contain less^than 260mg'/k'g total mWctity •'*•'• . :.•- • -"

WGUUTCD IMZAHOOUS COttSTH
Coflf»mon Hj«»a • *
Aldca-ta
.Mfthylpwjlhioo
•rNlphthyl2.|hk>urea - - 	
Nickel
Cyanides (Total)' .
. Cyanides Wme'nabiol' t "
Nickel s .. .
Nlcotlna and sails
Nitric oxW«
p-Nitrwniiin« ' -.,-..
Nitrogen dlovida .
Nitroglycerin
N-NitrbsodimethylarninQ
N-NitrosornethylvlnVlaminB "

Octamsthylpyrophosphoramlda
Osmlurn tetroxlde" - ~" ""'*' "*.~ .'•" •
-•Endothsll - . -. .'
Parathfon * "
Mercury. • • : •;.. _•
Morcury " • ' . ' '."• • •:':'—' ' 	 "... .'
Mercury " " . '.' '' " ' "• ' '
Mareury • -
i
lUtUT
CAS'HunlK'
'116-063
29B-00-0
ga.gs-4
744Q02"O
67 12-5
57 12.5
744002-0
. 54-1 1-6
10102-43-9
'. 100-01.6
- 10102-44-0
SS-63O
62-75-9
4S49-40-0

•152.16-9
20316-12-0
146-73-3 .
' 66-38-2 '
•7439-97-6
7439-97-6 '
7439-97-6'
7439-97-6 '

V/ASIEWATCRS
Covcntration M m^n\
a* Technology Co»6*
(WnOXw CHOXO) ft> CARBH. or
" WON
OOU , 	 ,„.,,,
tWETOXorCHOXDIIbCABBN;or .
INCIN
•- -398
12
0.86 •
398
(WETOX or CHOXDI fb CAflOH; or
. INCIN -'
ADGAS
• . 0.028
- ADGAS ". ' "
CHOXD: CHREO; CARBN; BIOOG; or
INCIN .
0.40 ' .
(WETOX or CHOXDI fb CARBN:' or '
INCIN
'CARBN; or IHCIN - r
' RMETUorRTHRM:
•(WETOX or CHOXD! fb CARON; or "' .
• • ' " ' INCIN - • . • '
0.014 " . ' '
• ... NA '•'-.'• -.
NA" .' '.•'-'•• -'•
NA • '-; • •_.- -;•••
... i- •
; NA '' ' "-.
".* * ""-' « 	 ' " "
"~ IWfWASTfSvATCBS
, , Conctntrnicniome/lo^, ,,_
wtturacin'ma/nar^ " ~
• IHCIH

INCIN.

690 -,
! '." 30

~ 	 ~ 	 '• 	 • * ; '
INCIN . •' ""'

'28
ADGAS
. '. CHOXO; CHRED; or CMBST
."••'" 2.3 " • :
	 " ' '• •'•INCIN'-i i---"' •'"•



- .CMBSf " '•'. .'•

•.. • -.' IMERC;' of RMERC •-•'•;;••
". . ;".;• ';••;•'" RMERC ••?- '• : ••:"-
".' • ' .' •'•-•:• 0 20 fng/l TClr '•" .'"}..-
• •'•-. %'o.OJ§:,mg/ITC'lP.. .-•'. " .
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-------
 P093-
 P094
 TO95 '
:P096
 P098
                   •' 'Waste Descrlptlon-and Treatmem/Regulatory Subcatogory'
                                                                               TREATMENT STANDAflDS FOB HAZAR'DOUS WASTES. •..
                                                                                          RECULATED HAZARDOUS CONSTITUENT
             All P092 Iphtnyl mercuric acetate) wastewaters
             Phenylthiouia'
             ' Pnorate
            .Phosgene _.:.
                                                                                             Common Name
                                                                                                                                                Concentration In mgfl1;

                                                                                                                                                 or Technology Code*
Phosphlne


Famphur


Potassium cyanide.
s . . 	







Mercury •
Pfcenylthlouea
"PhoratB ".
Phosgene ' "
.PiiospWna • ." .
Famphuf . '
Cyanides (Total)

                                                                                                                                                                       Concentration in mo/kfl*
                                                                                                                                                                     unless noted as''mo/I TCIP'
                                                                                                                                                                         or Technology Code
            Potassium silver cyanide  ''"
                                                                              " Cyanides (Total)!
                                                                               "™™"""^""^^.^^

                                                                               Cyanides Wnienablel


                                                                               Silver
            Ethyl cyanlda (Propanenltrile)


            Propargyl alcohol  "
                                                                  Ethyl cysnids (Propsnsnltrile!
                                                                               fropargyl alcohol


                                                                               «M«»^


                                                                               Selenium
                                                                                                                            ! iWETOX OT'CHOXBl ID CARBN; or- ,

                                                                                                                                         INCIN
                                                                              Cyanides (Amenable)


                                                                              Stiver
                                                                                                                                        'CHOXD; CHRED; CARBN; BIODG; or '

                                                                                                                                                   '  INCIN
                                                                                                                                                                   CHOXD; CHREDsbr CMBST
            ttychnJne and salts     '
                                                                                                                                         (WETOX Of CHOXO) (b CARBN; or

                                                                                                                                                     INCIM
            etrmthyldiihlopyropnospnan


            •traethyl lead  ' -
            VH*K^BB*^H"KBHHH

            elraeihylpyropriosphata:


            etranllrorneCriane^'. •:.-.-'.  .
                                                                Tetraeihyldlihlppyropnosphaia,
                                                                                                                                   CARBN;_o> INCIN


                                                                                                                                        0.69
                                                                                                                                                                           CMBST


                                                                                                                                                                   CHOXD; CHRED; or CMBST
                                                                                                                                      .  CHOXO; CHRED; CARBN; BIODG; or '

                                                                                                                                         ' '"   .    'INCIN-.  •
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-------
200   -    Federal'Register/-Vol.-60, No. 1 i Tuesday, January 3, 1995'/-Rules and Regulations':-;-:.-^-
        II!
        11
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                                                                        TREATMENT STANDARDS f OR HAZARDOUS WASTES
                                                                                  REGULATED HAZARDOUS CONSTITUENT
               Waste Description and Treatmem/Reoulatory Subcateflory1
                                                                                                                                        Concentration in mo/!'; '
                                                                                                                                         or Technology Code*
                                                                                                     Concentration In mo/kg'
                                                                                                   unless- noted-as 'mo/I TCU";
                                                                                                      or Technology Code •
                                                                                                                                   (WETOX or CHOXD) Ib CAR8N; or
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                                                                                                                                  •- (WETOX- or CHOXD) (b CARBN; or
                                                                       . Cycloheiienone; alternate? standard lor
                                                                                                                                   (WETOX or CHOXD) (b CARBN; or
                                                                                                                 2303-16-4-  I    (WETOX or CHOXD) (b CARBN; 01
                                                                                                                                             INCIM
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                                                                       1.2*Olbromo-3-chloroprQpBne
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                                                                       Ethyl«n« dibromlda ll.2.QI6romoiithanel
                                                                       Olbroftiomtthtne '  •
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     m-OlcMorobelueni
o-Dlchlofoben;«ne

(n-Olchlorobenzene
'. I  P-Olchlorob«men«

-------
                                                                                                                                               '*"
                                                              iKMuaa swxwsa ron HAJAJUXHB VMSHS
•
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— •--'•
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l.l-DlcMwoathylena • . ••*•'• • , '.' " 	 	 	
1,2-OIchteroalhylenj '.•-.. 	 " .•


Z.4rDlchl«oph«nol ..' ' "' . " •".- .
"2,6-OIchtorophenof ' •.'"'„.' ' - :" '_ '*. •_" .
1',2-DIcftloropropana ' ' . ' " - „ " ' ' '
"V,3-bichloropropylanav - -•' , . • . • . ' •
^ ,:-, •',.-;-..• . - '- •..'--• :. .,.-.•.'.-•, -t. ,
j*M^fiiii» ••••-•;:-. ;;; • . V, ._ • ••
' N.M'-blethylhydrailra "'',•-''' '""?'•
'O.apiBltiylSHna'thyldlthlophotphau' ' • - •• ' • ' - -
.'DIMhyl'phtluW* ' • •'•",. ' ' : ..-; : •
Dltttiyl itllbMtrol .- ' •'',•". •"'-'. "..'':"-.•••.•.
i . -• . -.-, .'. ..,......„..,.,..,..,. .. . . - • ..
' WhydroMfrola . -c- . ' ' • : ; •• »'• ; ' _'-' -.'•'_ ' '..
v^^-f.^ •?::,;•!•„•-;.. •
Olmelhytamlna . • _' : -'.•-f v _ '. . . '• \ . .

RtGMATCD KAZAnOOUS COilSTn
- Carman Hunt .
>««**«*• -; v
cis-1.4 DWAxo.2 txiUM
trjni.1,4.DleMwo.2-bu1w» ".
~ DtcMorodtduofometriana • ?-.%'„
LI-DlcMorociluna
1,2-Olchloroolh'mt '
Ll-Wchlbroothylana . """ "' ' '
lfsni.1.2-DicNoioiUliylono • •


2.4-OichloroDhanol ' ' " ' ' ' ' ' "
2;6-OicWorophi!nol . ,-"• *••••.>•••
I.J-DIchloropropana • ' - -- -
'ail^^chhxopropylan.' •-'•;':-:;- .'.
IransM.S-OlchlofoprotiylaM ~ 	 - •".•''
1.2:3,4-DiepoxVW!ana ;, • : ' 	 '• :'- <-. '--
• N.N.'.Dialliyihydratlrja • •
t
O.O-Olatnyl S-mathylwthloptiosphato • •
Dldliyl phlhaiata ' ., •
Dlaihyl alllbastcol '••.-. ; /,,•'_. •."•• ••
Dlhydrosafrots ' . ; ; •• •' '
S.S'-OIrnathoxybenzldlne • '" - , •
Dimethylamlne ' - • • •
. . . -r: ..- ....". , ' - '• L
p-Dlmethylaminoazobenzena
VEMT
CAS'Kumtw
9*1-94 t
1476.11-5
764-4KT
75-71-8 •
75-344
107-06-2
75-35.4'
156-60-5

75-03-2
120-83-2
' 87-65-0'
78-87-5
10081-01-5'
"10061-02-6..
— 146'4-53.5
161S-80-1
. 3288.58-2
.84-66-2
66-63-1
94-58-6
- 119-90-4 -
; 124-40-3. -
. 60-11 i •
WASTnVATEBS ' * '• "
Conctotinionlnma/',"* .
orTKhnoIosvCoik' . "» ,
(WnOXorCKOXDHbCARW/or "
iiicm"
• (WETOXtx CHOXO) IbCARBN; or '
INCIN •
(WETOX or CIIOXDI Ib CARBN; or
INCIN - -
0.23 •' ' •••-•
0.059 :
0.21
' 0.025 ' '
.0.054

0.089 • .-'•
0.044: '
' '•' 0.044 '
• - . ' 0.85
0.638
'0.036 ' 	 "
(WETOX or CHOXD) (b'CARBN; of -'
•INCIN •
CHOXO; CHRED; CARBN; BIODG; or .'
•INCIN - - - -•'• •
• CARBN; or INCIN " -
- ' 	 0.20
. (WETOX or CHOXD) fb CARBN; or
INCIN . •
tWETOX or CHOXOi.fb CARBN; or -
INCIN ' •'•...•"•,-
(WETOX or CHOXDI'fb CARBN: or —
INCIN . -.. -.' —
• (WETOX or CHOXD) (b CARBN; or .••'
" • -O13 i- '•• •-'.'
• ^MWASTtWAmS- «— *
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• • • . • • '30; ;•• ..' • -

- 30 'v^-'. • - • . -
• . . >14-r .-.',,, ••"•:
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-------
—— •••— ««™

Waste Code
•"MMHHMMM^
'U094
U095
"•™«««™™«nni™»^™
U096 .
"••••"•••MHWM^™
U097
U098 ...
•."U099 '
•• uioi.;.
. U102 -
U103 .
• U105 '
. . U106-.
--U107 •-.
	 U'108'"'.


. U109
- ... -: .•. ..
.UNO . .
.- U1-11 -V
U112 .
U113
••• • ;.-t^
•• '"• . ' . : '
- • ''•"•'••'•'•,•.' •• ••• : ...
• ; - ' ^ '
... Waste Description and Treatment/Regulatory Subcetegory' .• ;
7,12-Dlme!hyll»m(a)amhracehe
3.3'-DlmethyiberuldIhe '.'•'•'
, alpha, elpha-blmelrtyl benryl hydroperoxld« ,. •
Dlmethylcarbamoyl chloride * ', ' •
l.l-DlrnethylhydrailrM . . .
Z,4-Olmethytphenot' . > .- ' •
Dimethyl phthalaw . .- •• • .••-"'••
Dimethyl tullatt • . .
•2,4-Dlnltrotoluene' -' . ' . •
2,6-Dlnltrotoluaiw - .
D^rvoctyl phttulatt .
1,4-Dtoxaiw - . . ;;- .
•. , • ;' ..••'•• ;" . " ' • . .
. ••'-. ' ••", ' ' ' .' '•'•.'-..', ••-'
..'•.•-"•« •? * ' ' ' ' .-

DtpTOpylMTlIn*! - .' •-•t.. i . ,-"-,., ' "
Dwvptopy f rt tTOSvnlnii '-•'-••.*'.'•..-.,.. •" " *
Ethyiaca'tatt" • •• • ! .-."'-' . " • '. • .
Ethyl acrytat*:- • . ' • - .-. ""• '.' : •; ' • •• • '.' -.'.
EthylenaWjoltrilocarbamlff acid aalti and asters ';-..•: .. '• . -
- , . . " ; v ' '•' . • '."••'.'•' . \

. .'- REGUUTED HAZARDOUS CONST
. • Common Name
. 7,12-Dimethylt>ent(9)anthracen>
™«^<™°> . , : .
;alpha, alpha-Dimellivl benjyl hydroperoxlda "
Olmathylcaibamoyl chlorlds , '
• 1,1-Dlmethylhydrulne . . ' • - .
,1,2-Olmethylhydruine ' .
2.4-Dlm«thylpheno) . ...'"'• ' .' '
Dimethyl phthalate . ' :
Dimethyl sutfata , - . " "
2,4-DlnltrotoluerM
Ol-n-octyl phthalata'
1,4-Dkwane . -

1.4-Dloxane; attemiie1 standard for '
nonwastewaten only
1,2-Olphanylhydrailiia
1,2-Dlphanymv*ajln«;alternata«atand'afd • - -
for wastewatm only ' , .
Olpropylamlna". "•:••':".• ".•••' '•-.{••. ". . '•
Ol-n-propylnltrosamtne. ";; . .'-..".. ,-"•.,.'. _ '.T
Ethylacetata -'' • " '.". •;. ;
Ethyl KryltuvV I'!'":-' '•"' . ':•...
Ethylentblsdithlocarliamlc acid "•'.•:„-;•.. ..
^^3
BASTES
ITUENT
CAS' Number
. 57-97-6
...119-93-7
- 80-15-9
. '.79-44-7 . .
• 57-14-7 '; .
640-73.8
10S-67-9
131-11-3
77-78-1
- 12M4-2
606-20-2
117-84-0 •
• 123-91-1

. 123-91-1
.-,««..;.
122-68r7.. '
. V142-84-.7 '
'.', 621-64-7
141-78-6
'lio-88-6 '.'"
:ii'«^..
-• . - ,' V- ' .'' . . .

WASTEWATERS
Concentration In mg/l';
/ or Technology Code*
. (WETOX or CHOXD) Ib CARBN; or
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0.017 ' .
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290 .*
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Federal Register /Vol. 60. No. 1 ^Tuesday. January 3. IBM / »

-------
290    "   Federal Register 7 Vql: GO/ No.  1  / Tuesday. January 3, 1995 7. Rules 'anS^Regulations    •': /   - •- -V.'!: / ;
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                                                              •   TREATMENT STANDARDS FOR HAZARDOUS WASTES
Waste. Coda.
! '.U226 .

U228
0234'-'
0235' '..
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0237
0238
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...V. '. , '.WaMa'.OeMrtpUonandTre'atmant/Reo^atc^Subcategory',.. ... _ ,
l.l.l.Trtehloroethane- •'•'.•-. '."
t.'W-TrichlorMthane . .. - .
.Trlchlofoethylerm - . • . ,' . '
'I'AS-Trtnltroboruime'^- •'•- '' ''• • .'•• ' .. " ' ' • • i • •• .V • .-.. -
trls-l2,3-Dtbromopropyl)-phosphat6. , - •
Trypan Blua • ' " " -" ••
..'••••; •> . • • • . -
OrMtl 'mustard '". " '•'• ' .•
..-.-..'.' .1 . . " ," ' ' '-'' '' '•
.Orethan»(Elhylcarb«maia) • .; - • ... . ., ..;
Xyfener ' ' '....'.:";''
2.4-0 (2.4-DIchlorophenoxyac«leacld) *- ' '.. • •
•2,44> (2.4-Dldilw0pti«i»xvacatlc add) :. . .
talts ami «sterj '.'-••••
HaxacMofopropylana ."..',• .. .'
TWram . < ' . . .
Cyanogwi bromlda ' • . • . • - " ' '
Wwtirin, & ufu. wtwn prtMnt it coneantrttlont of 0.3% or lau
Zne plHMpWda. Zn,P|. wtwn presant tt'eoncentritlona of 10% of laa»
o-ToiiA«» • - • ' .^.;. .:'„..'.;,'•.' .''-..'. ' ' ". '
p-Totuldltw .-•-'.-•" :....'..,•.•,•: ',../. ..:. •:..*;..'
2-Ell»iiyalh«noI : . '"'.''. ;':-* ; ".' '.' '•' '; '
• . 'REGULATED HAZAROO'U'S'CONSTITUeNT
^ ••-•.. ^ - . , . Common Nama . ' ... -;
'1.1.1 Trtchloroelhana. .
1,1.2-frichlordatHana
Tr'lchloroaihylana . 	
f ,3,5-Trlnltrobaniana' • • ' '. ? " •

'Trypan Blua '• -'•'.' '
Oracll muataid ' ' "
Uralhana fEthyl carbamata)
Xylanas^nlxad (sorrier* ' ' ' "
(sim of o-, m-. and p-xylana coneantratlona) .
2.4-D (2.4.DlcMoroph«noxyacatlc acid) .

Hexachloropropytane
TNram, . - • • .
Cyamgan bromhte
MathoxycNor . ' .
Warfarin ...

Zinc Phosphlda '' •'•'.'•
o-Totuldirw. • • . ., ,. . . " '' " ;
p-ToIufdlrM' ' "•- .'. .- •-
jt-Ethoxyathano! . . " . !.':'"

• CAS'Numbar

' _ 79.00.5- '.
' ^941-A'"..
.99-35-4 '•.
126i72-7
- 72-57-1
• 68-75-1
61 79^8 ,'
. 1330.20-7

.". •; MA-- ..
1888-71-7
137-26-8 •
606-68-3
72-43-5.
" 81-81-2 .
W14-S4-7
' 95-53-4
. 106-49-0
•11 0-80-5

' ' WASTEWATERS
- . Concemr'allonlhrng/l1;'' '
. .or Technology CoiSa'" ' '. ' '

: ' ' ' ' 6.054 •'
'• 0.054 '-
(WETOX or CHOXD) fb CARBN; .or .:
;---- 0.11 - • •;•
(WETOX or CHOXDI fb CARBN: or
" ' • ' INCIN • •
(WETOX or CHOXD) fb CARBN; or
» . • INCIN ' . • •
(WETOX or CHOXD) fb CAR8N;'of
INCIN
.0-3'2 .^'.''. '. ':
. ' 0.72 '
(WETOX or CHOXDI fb CARBN; or
. • . ' 0.035
• • (WETOX or CHOXD) fb CARBN; or
INCIN
CHOXD; WETOX; or INCIN
" 0.2S •
' (WETOX or CHOXD) fb CAHBN; or
; INCIN
CKOXO; CHREB; or INCIN . -
' INCIN; or CHOXD fb (BIOOS or
. . CARBN); or BIODGfb CARBN.
INCIN; or CHOXD n> (BIODG or
. -: , .CARBN); or 8IODQ f b'CARBN ' '
\ 'INCIN; or CHOXO Ib (BIODQ or 1 '.•
CARBN); or BIODG fb CARBN '. .


• • • Concentra'tlpn In'mg/Vg* -. . .-: -
urilass notad'as 'mg/I TCti";. -":. •
- " or Technology Code ' • •'• :-•

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'se:o: : ; :• "
.., -- . --"iNCIN.

INCIN i
• '^'IMCIM' •'•'•.


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rNCIN .
'-' '• 30-* .'...-' -
. ' . .INCIN' ,-'••
. ; •
" " . CHOXD; WETOX; Or INCIM
• .' • 0.18 -.-. '•• .- '.
-. -. :'' ' - . CMBST \ '" • • •' -
CHOXO'* CHRED* or INCtN
INCIN; or Tlwrmal Oaslructlon .
' INCIN; or Tlwmal Destruction.
•>--',
:.." ••' » CMBST . ..- ' :.'' '

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 302      " Federal Register / Vol.-60, No.  1 / Tuesday. January 3, 1995 / Rules and. Regulations   y   .   ,T:t•
                                                                                         .' 9'.
 Notes to Table             .......   ."
   5 Tho ivaste descriptions prox'i'de'd in this..
 "table do not replace waste descriptions in 40,
 CFR part 261. Descriptions of Treatment/   .
 Regulatory Subcategories are provided, as •• .•
 needed, to distinguish between applicability
 of different standards.    .  .'  '%".'"" '.
   = CAS means Chemical Abstract .Services.
 \Vhen the waste code and/orregulate'd
 constituents are described as a combination •
 of a chemical with it's salts and/or esters, the
 CAS number is given for the parent   '     •
 compound only.         '   "'.'"'    •
   3 Concentration standards for wastewaters.
 arc expressed in mg/1 are based_on analysis  ,
 of composite samples.  '      ",      .  - •
   * All treatment standards expressed as a
 Technology Code or combination of •  ;   .
 Technology Codes are explained in derail in'
 40 CFR part 268.42, Table 1—Tecluiology
 Codes and Descriptions of Technology-Based
 .Standards.                 '   ,  •  • •
   9 Except for Metals (EP or TCLP) and
 Cyanides {Total and Amenable) the.
 nonwasto water treatment standards   .
 expressed as a concentration.' were '• .'
 established; In part, based upon incineration
 In units operated In accordance with the,  -
 .technical requirements of 40 CFR part 2C4.
 subpart O, or part 265, subpart O, or based
 upon combustion in fuel substitution units
 "operating In accordance with applicable.
; technical requirements. A facility may •
 comply with these treatment standards.
" according to provisions in 40 CFR 268.40(d).'
 All concentration standards for  >'
 nonwastewatcrs are based on analysis of grab,
 samples. *             '         '      ''••
   6 Whuro an alternate treatment standard or
 set of alternate standards has been indicated,
 a facility may comply with this alternate
 standard, but only for tho Treatment/
 Regulatory Subcategory or physical form (».e.,
 xvaslowater and/or nonwastewater) specified
 for that alternate standard.
    7 Both Cyanides (Total) and Cyanides   . .;
  (Amenable) for nohwastewaters are to be/ .
  analyzed using Method 9010 or 9012, found
  in "Test Methods'for Evaluating Solid Waste/
  Physical/Chemical Methods"* EPA '. - V:   ,
  Publication SW-846, as incorporated by ';"
  reference in 40 .CFR 260.11> With a sample  ';
 • size of 10 grains and a distillation time of one
  'hourand 15minutes.  \.•'•.••':•'  •'••.
  '  Note: NA means not applicable.  .   ' V ••
  *    *.."*•   *.'*.--  , •.     .»  •'.

    6. Section 268.42.is amended by  :
  revising the entry, "CMBST" in Table I •
  to'read  as follows:.   "      .-. ,-

  § 268.42  Treatment standards expressed
  as specified technologies.    .    ,
  TABLE  1.-^TECHNOLOGY  CODES-AND
  •  DESCRIPTION    OF   TECHNOLOGY-,
     BASED STANDARDS   \    ;  .    .. ;

  Technology  Description of technotogy-based
   •  code  ..   '    •    'standards •.. •.  '•
  CMBST "    Combustion in incinerators, boil-
 • •':: •' ,   .'  •"• ers, or indostriaKfufnaces op-
•   •:.-',   'crated in accordance with the
    •'•   •    '•   applicable requitements.of 40
             v.. CFR part.264.-subpart O; 40
            • ""CFR part 265, subpart O; or
          ' •'   "40 CFR part 266, subpart H.
     7. Section 268.48 is amended by
  adding footnote 5 to the entry for •  •  .'
  Vanadium and revising the foohiote to
  read as follows;. ;""  /.   '•    .  .-'•.'  ••"•••
 §268.48  Universal Treatment Standards. •  :.
". §268.48 TABLE
'• •? Vanadium/and sanc.are cot "undeTiying.
 hazardous constituents'* in characteristic   '• .' •
 wastes, according .to the definition at 268;2{i).
   Note: N A means not applicable. .':,••:'•

   8.' Appendix X to part 268 is amended   :
 by revising Certification Statement B to~
 'read as follows:  :       \ .'" .. " ••  ..,-'.'••

, Appendix X to Part 268--   ;   ; ''•:
 Recordkeeping, Notification, and/or   '.
 Certification Requirements. .       •':~%

 *    ' *   ''••.*•'..  *  •'*.'.',.•" ;r ;."...".~" ,

 Certification Statements '.  -..  .,.'  v ,.'_'• ;'•..".
• *     *''".'• .?''*'.''* -\c'-iii(:••:••'-, '• '    ••'••:••'•'

   B. I certify under pehafty of la\v that  •
 I personally have examined and am;-   .;
 familiar with the waste and that the lab ;
 pack does riot contain any wastes  : ;'••• • '
 identified at Appendix IV to part 268.1 ..*.
 . am aware that there are significant  "
 penalties for submitting a'false  ; • '••
 . certification including possibility.of fine
 •or imprisonment: •' .>'..,.'  •  '.'"•
                                                "* . '•  •*  '  '*
                                           |FR Doc 34-32118 Filed 12-3rP94; 8:45 am{

                                           BILLING CODE "»56»-«0-4P   '.,  ;,  ',    .•,:;••"•-

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