Thursday
 November 19, 1998
Part IV



Environmental

Protection  Agency

40 CFR Part 261
Hazardous Waste Management System:
Identification and Listing of Hazardous
Waste, Solvents; Final Rule

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64372    Federal Register/Vol.  63,  No. 223/Thursday, November 19, 1998/Rules and Regulations
ENVIRONMENTAL PROTECTION
AGENCY

40 CFR Part 261

[SWH-FRL-6185-3]

RIN 2050-AD84

Hazardous Waste Management
System: Identification and Listing of
Hazardous Waste Solvents

AGENCY: Environmental Protection
Agency.
ACTION: Final decision.

SUMMARY: The U.S. Environmental
Protection Agency (EPA) is issuing a
final decision not to list wastes
generated from the use of 14 chemicals
as solvents as hazardous under the
Resource Conservation and Recovery
Act (RCRA). The determinations in this
rule are limited to specific solvent
wastes. This rule is a determination
only that the solvent wastes considered
will not be added to the list of
hazardous wastes and is not a
determination that the underlying
chemicals are nontoxic in all
circumstances in which they are used or
discarded.
DATES: Today's final decision will
become effective on December 21, 1998.
ADDRESSES: Supporting materials are
available for public viewing and
photocopying in the RCRA Information
Center (RIC), located at Crystal Gateway
I. First Floor. 1235 Jefferson Davis
Highway. Arlington, VA. The Docket
Identification Number is F-98-SLDF-
FFFFF. The RIC is open from 9:00 a.m.
to 4:00 p.m., Monday through Friday,
excluding federal holidays. To review
docket materials, it is recommended
that the public make an appointment by
calling (703) 603-9230. The public may
copy a maximum of 100 pages from any
regulatory docket at no charge.
Additional copies cost S0.15/page. The
index and some supporting materials
are available electronically. See the FOR
FURTHER INFORMATION CONTACT  section
for information on accessing them.
FOR FURTHER INFORMATION CONTACT: The
RCRA/Superfund Hotline, toll-free, at
(800) 424-9346 or at (703) 920-9810.
The TDD Hotline number is (800) 553-
7672 (toll-free) or (703) 486-3323 in the
Washington, DC metropolitan  area.
  For technical information on the
RCRA hazardous waste listings, contact
Ron Josephson or Robert Kayser, Office
of Solid Waste (5304W), U.S.
Environmental Protection Agency, 401
M Str.eet, SW, Washington, DC 20460.
The telephone number is (703) 308-
8890.
 SUPPLEMENTARY INFORMATION : There are
 no regulated entities as a result of this
 action.
   The index and the supporting
 materials are available on the Internet:
 Follow these instructions to access the
 information electronically:
 WWW: http://www.epa.gov/epaoswer/
   hazwaste.htm#id
 FTP: ftp.epa.gov
 Login: anonymous
 Password: your Internet address
 Files are located in /pub/oswer
   The contents of the preamble to this
 final rule are listed in the following
 outline:
 I. Legal Authority and Background
  A. Statutory and Regulatory Authorities
  B. Existing Solvent Listings and the
    Regulatory Definition of Solvent
 n. Summary of Proposed Rule
  A. Determinations Not to List Solvent
    Wastes as Hazardous Waste
  B. Summary of Risk Assessment
    Supporting the Proposed Rule
 m. Peer Review of Calculated f oxicological
    Benchmarks
 IV. Summary of Response to Comments and
    Rationale for Final Rule
  A. Data Collection
   1. Representativeness of Industry
    Characterization
  2. Engineering Site Visit Reports
  B. Methodology
   1. Definition of "Solvent'
,   2. Lack of Sampling and Analysis
   3. Consistency of Methodology With Other
    Listing Determinations
   4. Plausible Mismanagement Scenarios
   C. Risk Assessment
   1. Surface Impoundments
   2. Tank-Based Management of Wastes
   3. Multiple Solvents
   4. Comparison with HWIR Exit Levels
   5. Environmental Damage Incidents
   6. Spills, Leaks, and Overflows
   7. Non-Aqueous Phase Liquids
   8. Risk Modeling Parameters
   9. Comparison with Results of Air
     Characteristic Study
   D. Listing Determinations
   1. General Comments
   2. Sufficient Regulation of Solvents
   3. Waste-Specific Rationales and Response
     to Specific Comments
 V. Regulatory Requirements
   A. Regulatory Impact Analysis Pursuant to
     Executive Order 12866
   B. Regulatory Flexibility
   C. Unfunded Mandates Reform Act
   D. Executive Order 12875: Enhancing
     Intergovernmental Partnership
   E. Executive Order 13045: Protection of
     Children  from Environmental Health
     Risks and Safety Risks
   F. Environmental Justice E.O. 12898
   G. Paperwork Reduction Act
   H. National Technology Transfer and
     Advancement Act
   I. Executive Order 13084: Consultation and
     Coordination with Indian Tribal
     Governments
   J. Congressional Review Act
I. Legal Authority and Background

A. Statutory and Regulatory Authorities
  The Environmental Protection Agency
(EPA) conducted this investigation and
listing determination under the
authority of sections 2002(a), 3001 (a),
(b) and (e)(2) of the Solid Waste
Disposal Act (42 U.S.C. 6912(a), and
692 l(b) and (e)(2)), as amended by
various other laws, the most
comprehensive of which was the
Hazardous and Solid Waste
Amendments (HSWA) of 1984. These
statutes are commonly referred to as the
Resource Conservation and Recovery
Act (RCRA) and are codified at Volume
42 of the United States Code (U.S.C.),
sections 6901 to 6992 (k).
  Section 3001(a) of RCRA, 42 U.S.C.
6921 (a), requires EPA to promulgate
criteria for identifying characteristics of
hazardous wastes and for listing
hazardous wastes. Section 300 l(b) of
RCRA requires EPA to promulgate
regulations, based on these criteria,
identifying and listing hazardous wastes
which shall be subject to the
requirements of the Act. Section 1004(5)
of RCRA, 42 U.S.C. 6903(5), defines the
term "hazardous waste." There are two
types of hazardous waste. First,
hazardous wastes are those solid wastes
which  may cause or significantly
contribute to an increase in mortality,
serious irreversible illness, or
incapacitating reversible illness.
Second, hazardous wastes are those
solid wastes which may pose a
substantial present or potential hazard
to human health or the environment
when improperly managed. Id.
  EPA's regulations establishing criteria
for listing hazardous wastes are codified
at Title 40 of the Code of Federal
Regulations (CFR) 261.11 (40 CFR
261.11). Section 261.11 presents three
criteria by which EPA identifies wastes
as hazardous.
  First, solid wastes may be classified as
"characteristic" wastes if they exhibit
any of the characteristics of hazardous
waste identified at 40 CFR 261.21-24
(i.e., ignitability, corrosivity. reactivity,
ortoxicity).
  Second, solid wastes may be listed as
acutely hazardous if they are fatal to
humans at low doses, lethal in animal
studies at particular doses designated in
the regulation, or otherwise capable of
causing or significantly contributing to
an increase in serious illness.
  Third, solid wastes may be listed as
hazardous if they contain any of the
toxic constituents identified in
Appendix VIII of 40 CFR part 261 and
the Agency concludes, after considering
the eleven factors enumerated in 40 CFR
261.11 (a) (3), that the waste is capable of

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           Federal Register/Vol. 63, No.  223/Thursday,  November 19, 1998/Rules and Regulations    64373
 posing a substantial present or potential
 hazard to human health or the
 environment when improperly
 managed. A substance is listed in
 Appendix VIII if it has been shown in
 scientific studies to have toxic,
 carcinogenic,  mutagenic, or teratogenic
 effects on humans or other life forms.
 Today's listing determination has been
 made pursuant to this third set of
 criteria.
   As part of its regulations
 implementing section 300 l(b) of RCRA,
 EPA published a list of hazardous
 wastes that includes hazardous wastes
 generated from nonspecific sources (F-
 wastes) and a  list of hazardous wastes
 from specific sources (K-wastes). These
 lists, published at 40 CFR 261.31 and
 261.32, respectively, have been
 amended several times.
   Persons who generate, transport, treat,
 store, or dispose of wastes listed as
 hazardous must do so subject to Federal
 requirements under RCRA. Facilities
 that must meet the hazardous waste
 management requirements, including
 the need to obtain permits to manage
 hazardous wastes, are commonly
 referred to as RCRA Subtitle C facilities.
 EPA standards and procedural
 regulations implementing Subtitle C are
 found generally at 40 CFR parts 260
 through 279.
   Solid wastes that are not hazardous
 wastes may be disposed of at facilities
 that are overseen by State and local
 governments. These facilities are
 referred to as RCRA Subtitle D facilities.
 EPA regulations affecting Subtitle D
 facilities are found generally at 40 CFR
 parts 240 through 247, and parts 255
 through 258.
   Section 3001 (e) (2) of RCRA requires
 EPA to determine whether to list as
 hazardous several specified wastes,
 including solvent wastes. The
 Environmental Defense Fund (EDF) and
 EPA entered into a consent decree to
 resolve issues  raised in a civil action
 brought by EDF (EDFv. Browner, Civ.
 No. 89-0598 (D.D.C.)) in which the
 Agency agreed, among other things, to a
 schedule for making a listing
 determination on spent solvents. This
 listing determination is to consider
 spent solvents, still bottoms from the
 recovery of these solvents,, and spent
 solvent mixtures when the following
 chemicals are used as solvents: cumene,
 phenol, isophorone, acetonitrile,
 furfural, epichlorohydrin, methyl
 chloride, ethylene dibromide, benzyl
 chloride, p-dichlorobenzene, 2-
 methoxyethanol, 2-methoxyethanol
acetate, 2-ethoxyethanol acetate, and
cyclohexanol.
  For an additional set of seven
solvents, EPA agreed to conduct a study
 and issue a final report by August 30,
 1996. This study, which EPA completed
 on August 22, 1996, discusses the
 wastes associated with the use of the
 materials as solvents, the toxicity of the
 wastes, and a description  of the
 management practices for the wastes.
   Solvent uses are found throughout
 various industries and, thus, would fall
 under the category of wastes from
 nonspecific sources (F-wastes) if listed
 in 40 CFR 261.31. In fact,  wastes
 designated F001 through F005 are
 various wastes from solvent uses of a
 number of chemicals. In today's action,
 EPA has decided not to amend 40 CFR
 261.31 to add wastes generated during
 the use of the 14 chemicals of concern
 as solvents.
   EPA emphasizes that the
 determination not to list these wastes
 only means that the Agency has found
 it is not appropriate to list as hazardous
 the wastes across broad industry
 categories that could result from solvent
 uses of the 14 chemicals. As will be
 more fully explained below, EPA  did
 not find that solvent uses for these
 chemicals, in general, produce
 hazardous wastes that require listing.
 Many of the wastes  examined are
 hazardous already because they are
 characteristic wastes under 40 CFR part
 261, subpart C, or contain  other solvent
 wastes currently listed as hazardous. In
 addition, some of the chemicals may
 produce wastes that are hazardous when
 used in ways other than as solvents,
 perhaps as catalysts, feedstocks or other
 uses in chemical manufacturing
 processes. Solvents use simply does not
 constitute an appropriate way to
 designate these chemicals as a
 hazardous waste category under RCRA
 for wastes from nonspecific sources.
 Particular industrial wastes from these
 chemicals might be hazardous, but such
 wastes were not examined in this
 determination.
 B. Existing Solvent Listings and the
 Regulatory Definition of Solvent
  Five hazardous waste listings for
 specific solvents have been promulgated
 to date: F001, F002, F003,  F004, and
 F005. These are found at 40 CFR 261.31.
Today's decision applies the same
 criteria for defining solvent wastes as
 are applied to these existing solvents
listings. These criteria are explained in
the Federal Register of December 31,
 1985 (50 FR 53316) and are also
consistent with the requirements of the
EDF Consent Decree.
  The December 1985 document
amended the solvent listings to include
spent solvent mixtures when the
solvent, before it is used, contains 10
percent or more of total listed solvents.
 The original listing included only the
 technical grade, practical grade or pure
 form of the solvents when used. This
 threshold level was considered by the
 Agency to be well below the minimum
 solvent concentration typically used in
 solvent formulations and was designed
 to bring the majority of listed solvent
 mixtures used in commerce into the
 hazardous waste management system,
 while excluding dilute mixtures or de
 minimis concentrations.
  In addition, the document issued
 several clarifications to the original
 listings. First, the listings apply to
 "spent" solvents—those that are no
 longer fit for use without being
 regenerated, reclaimed, or otherwise
 processed. (See 40 CFR 261.1(c) (1) and
 (4); 261.2(c) (3) and (e)). Second, the
 listings cover only those solvents used
 for their solvent properties—"to
 solubilize (dissolve) or mobilize other
 constituents." These include solvents
 used in degreasing, cleaning, fabric
 scouring, as diluents, extractants,
 reaction and synthesis media. The
 document stated that the listings do not
 cover wastes from the processing of
 products where a chemical that might
 be used as a solvent is, instead, used as
 a reactant or where a chemical is used
 as a solvent only as an ingredient in the
 formulation of a commercial chemical.
 This latter category would include
 chemicals used as a solvent in paint
 formulations to dissolve the paint itself.
 These uses do not generate "spent
 solvent" wastes. The wastes of concern
 for these products would be the
 production process wastes or wastes
 from the use of the product, not the
 solvent itself.
  This approach is also consistent with
 the requirements of the EDF Consent
 Decree. This is because the consent
 decree identifies a subset of solvent
 wastes that are potential candidates for
 listing and specifies that the listing
 determination applies to "spent
 solvents," a term that tracks the
 language of the existing listings.
 Moreover, this approach had been the
 longstanding approach of the Agency to
 dealing with solvent listings at the time
 the Consent Decree was negotiated and
 should be interpreted as representing
 the understanding of the parties.
  This approach, whereby EPA has
 limited the scope of this rulemaking
 through this focused definition of
solvents subject to the listing, is  a
reasonable interpretation of RCRA and
 is consistent with EPA's historical
treatment of solvent listing descriptions.
Use of the definition has allowed the
Agency to place reasonable limits on the
scope of its listing investigation for this
rulemaking. RCRA3001(e)(2) directs

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64374    Federal Register/Vol. 63, No.  223/Thursday,  November 19,  1998/Rules and Regulations
EPA to make a listing determination on
"solvents," but provides no further
direction on the meaning of that term.
EPA, therefore, has the discretion to
reasonably define the scope of the
listing determination. Given the
ubiquity of solvents, the great variety of
uses and the huge differences in the
composition of the waste streams, EPA
could not gather the evidence to list
"solvent wastes" as a general category.
Under the Agency's regulations at 40
CFR 261.11 (b), wastes may be listed as
a category if they are "typically or
frequently" hazardous. EPA could make
no such findings for "solvent" wastes in
general and, therefore, has reasonably
focused its investigation and listing
decision.
  As noted above, the existing solvent
listings are limited to spent solvent
mixtures when the solvent,  before it is
used, contains 10 percent or more of
total listed solvents. While wastes from
this use threshold were the primary
focus of today's listing determination,
EPA also considered in its evaluations
the few solvent uses that were reported
to be below the 10 percent threshold.
  In a previous proposed hazardous
waste listing for wastes from the
production of dyes and pigments (59 FR
66072, December 22, 1994) EPA
presented the general approach the
Agency uses for determining whether to
list a waste as hazardous pursuant to 40
CFR 261.11 (a) (3). The discussion
focused on the selection of waste
management scenarios used in assessing
risk and the use of information on risk
levels in making listing determinations.
This approach was further developed in
EPA's listing for petroleum refining
process wastes (proposed rule published
at 60 FR 57747, November 20, 1995;
final rule published at 63 FR 42110,
August 6,  1988). EPA is employing the
same general approach in this final
rulemaking. Readers are referred to
these documents for a description of
EPA's listing policy. Also, section II.C.2.
of the proposed rule, "Risk
Assessment," contains a discussion of
how elements of EPA's listing policy
were applied in today's listing
determination.
  The following section contains a
summary of the methodology  used to
arrive at the no-list determinations in
today's document. For more details on
this methodology, see the proposed rule,
background document, and the response
to comments document in the docket.
EC. Summary of Proposed Rule

A. Determinations Not To List Solvent
Wastes as Hazardous Waste
  EPA proposed the decision not to list
the spent solvent wastes from the 14
chemicals noted above on August 14,
1996 (61 FR 42318). The Agency
determined that these wastes did not
meet the criteria for listing set out in 40
CFR 261.11. The proposed rule
presented the waste characterization,
waste management, mobility,
persistence, and risk assessment data
that were the bases for the Agency's
proposed decision not to list these
wastes as hazardous. Further details of
EPA's approach are presented in the
Hazardous Waste Listing Determination
Background Document for Solvents
(hereafter known as "Listing
Background Document") in the docket
for the proposal to today's rule.
  As explained in section II.B of the
proposed rule, spent solvents differ
from other listed wastes among EPA's
waste listings in that the solvents are
used in manufacturing and allied
processes rather than being the
principal waste streams generated by
manufacturing processes. In order to
characterize industrial solvent use, the
Agency sent out almost 1,500
preliminary questionnaires to cover the
21 total chemicals (14 from the listing
determination and seven from the
study). An additional 60 facilities were
surveyed on their use of these chemicals
as solvents through the chlorinated
aliphatics industry survey. EPA then
sent out a full RCRA section 3007
survey to facilities using greater than a
combined total of 1,200 kilograms of all
the chemicals-sf concern.
  The Agency consulted various
literature and reference sources, such as
Chemical Abstracts, general reference
books, the Agency's Toxic Release
Inventory (TRI) compiled under section
313 of the Emergency Planning and the
Right-to-Know Act (EPCRA), databases
compiled for various EPA programs
dealing with air and water pollution,
and information available from trade
associations. Of the 14 chemicals
involved in the listing determination, 11
were on the TRI. Use of the literature.
Chemical Abstracts, TRI, and other EPA
databases allowed the Agency to focus
on the industries that actually use these
chemicals as solvents. In addition, many
of these sources gave strong indications
as to when major uses of a chemical
were not as a solvent.
  Once the Agency narrowed down the
potential solvent-using industries, the
Agency developed a list of facilities to
survey about their solvent use. These
facility names and addresses were
obtained again from a variety of sources,
including TRI, trade associations, and
other Agency media program sources.
The Agency sent a short ("preliminary")
questionnaire to approximately 1,500
facilities inquiring about uses of any of
the 14 listing determination chemicals
as solvents and the quantities used.
  The Agency used the preliminary
questionnaire data to develop the large
questionnaire mailing list and to
organize site visits. The Agency also
made several hundred confirmatory
telephone calls to determine that
reported information was correct. The
data  from the preliminary questionnaire
showed the Agency several distinct
patterns of solvent use: facilities that
use large amounts of any of these
chemicals as solvent, those that use
small quantities as solvents, and those
that use none of the chemicals as
solvents. The Agency found that a
solvent use quantity of 100 kg per
month, or 1,200 kg per year, provided a
mathematically convenient separation
of those facilities who use large amounts
of solvent and those who use very little
and provided an indication as to which
facilities were likely to be large quantity
generators of hazardous waste based on
use of these chemicals as solvents.
Based on careful analysis of the data,
the Agency identified likely large-scale
users of these chemicals as solvents.
  The Agency then developed the large
questionnaire. This questionnaire
reconfirmed data on solvent use and
requested detailed information  on a
facility's solvent-using processes, waste
generation, waste management, and
waste minimization activities. The
Agency sent this questionnaire  to
approximately 150 facilities that
indicated to the Agency through the
preliminary questionnaire that
significant solvent uses of these
chemicals exist. The data obtained from
the questionnaire were applied  to the
risk assessment process described in
today's document as well as the
preparation of the background
document.
  To summarize the results, 4 of the 14
chemicals showed no use as a solvent.
The remaining 10 chemicals were
analyzed in the Agency's risk
assessment based on solvent uses found
by the Agency. For the 10 chemicals of
the required listing determination for
which there were solvent uses
(acetonitrile, 2-ethoxyethanol acetate, 2-
methoxyethanol, 2-methoxyethanol
acetate, cyclohexanol,  cumene,  phenol,
furfural, isophorone, and methyl
chloride), EPA found that the
management of residuals from the use of
these chemicals as solvents did not pose
a risk to human health or the

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            Federal Register /Vol. 63, No.  223/Thursday, November  19,  1998/Rules and Regulations     64375
 environment under the plausible
 management scenarios assessed. The
 data used as the bases for these
 determinations were presented in
 sections II.D through II.M of the
 proposed rule (61 FR 42327). Detailed
 information is also presented in the
 background documents supporting the
 proposed rule (RCRA Docket number F-
 96-SLDP-FFFFF).
   Specifically, none of the solvents
 satisfy the criteria for listing in 40 CFR
 261.11 (a) (3). For acetonitrile, 2-
 methoxyethanol, and methyl chloride,
 while risk analyses indicated some
 potential risk from air releases of these
 chemicals from onsite accumulation in
 open tanks, EPA believes this risk
 would not be significant because most,
 or in some cases all, of the
 nonwastewater residuals are already
 regulated as hazardous waste. For
 phenol, 2-ethoxyethanol acetate,
 furfural, cumene, cyclohexanol,
 isophorone, and 2-methoxyethanol
 acetate, the  risk estimates indicated that
 spent solvent residuals from the use of
 these chemicals as solvents do not pose
 a substantial risk or potential hazard to
 human health or the environment
 through the plausible management
 scenarios and pathways assessed.
   For the remaining four chemicals
 subject to the required listing
 determination in the EDF Consent
 Decree (1,4-dichlorobenzene, benzyl
 chloride, epichlorohydrin, and ethylene
 dibromide), EPA proposed not to list
 residuals from their use as solvents,
 because the data collected by EPA
 showed that these chemicals are
 extremely unlikely to be used as
 solvents. One of the chemicals (p-
 dichlorobenzene) is a solid at room
 temperature, and the other three (benzyl
 chloride, epichlorohydrin, and ethylene
 dibromide) are relatively reactive
 chemicals not well suited to solvent use.
 EPA's information showed that the very
 limited solvent use reported for these
 four chemicals is linked to bench-scale
 or experimental laboratory settings, and
 no significant solvent uses were found.
 For more detail see sections II.N through
 II.Q of the proposed rule (61 FR 42347)
 and background documents supporting
 the proposed rule (RCRA Docket
 number F-96-SLDP-FFFFF).

 B. Summary of Risk Assessment
 Supporting the Proposed Rule
  As described in detail in the proposed
rule  (see 61 FR 42322-42327), EPA
carried out various analyses to
determine the potential risk that might
arise from the disposal of the spent
solvent wastes under study.  In carrying
out the modeling for these assessments,
EPA used available data it collected
from industries using these solvents.
 The Agency used information gathered
 in the RCRA 3007 Questionnaires and
 site visits related to the waste
 characteristics, waste management
 practices, and potential pathways for
 release and exposure. EPA used other
 generic input parameters to fate and
 transport models to estimate the risk a
 waste might present under management
 scenarios known to occur. The data
 used in the modeling efforts included
 the concentrations and toxicity of the
 solvent constituents in the waste, the
 mobility and fate of such constituents in
 different disposal scenarios, likely
 exposure routes under these scenarios,
 and the location of receptors that might
 be exposed.
   The levels of receptor exposure
 estimated from modeling were
 compared with toxicological
 benchmarks to evaluate the potential
 health impacts. For noncarcinogenic
 constituents, EPA used reference doses
 for ingestion exposure (RfDs) and
 reference concentrations for inhalation
 exposure (RfCs); these are measures of
 acceptable daily intakes for a specific
 chemical. To assess the hazard to a
 hypothetical individual, EPA used
 hazard quotients (HQs). An HQ is the
 ratio of the modeled exposure (or dose)
 received compared with-the acceptable
 daily dose  (the RfC or RED). An HQ
 above one indicates that exposures may
 occur above acceptable levels. For
 carcinogenic constituents, EPA
 compared exposure levels to
 carcinogenic potency estimates
 (carcinogenic slope factors, or CSFs) to
 calculate specific risk levels. The
 carcinogenic risks results are expressed
 in terms of individual risk, reflecting the
 additional incidence of cancer that may
 occur in an exposed population. For
 example, a risk of 1 x 10~5 (which will
 be presented in this document as IE-OS)
 corresponds to a probability of one
 additional case of cancer for every
 100,000 people exposed.
  EPA used verified RfDs, RfCs, or CSFs
 when available in EPA's Integrated Risk
 Assessment Information System (IRIS).
 IRIS, which represents a consensus
 opinion of EPA health scientists, is a
 database of human health effects that
 may result from exposure to various
 substances found in the environment.
 For the chemicals that did not have
 complete verified IRIS data available (2-
 methoxyethanol acetate, cyclohexanol,
 phenol, and isophorone), EPA
 calculated provisional values when
 needed for use in the listing
 determinations.
  EPA performed a number of different
types of risk analyses. First the Agency
completed a "bounding analysis" to
screen out solvent wastes from further
consideration. In this analysis, the key
 input parameters were set to their
 "high-end" values (typically the 90th
 percentile point on the distribution of
 values available for each parameter). For
 solvent wastes that did not "bound
 out," EPA then ran a high-end
 "deterministic" sensitivity analysis to
 determine which high-end input
 parameters result in the greatest risk.
 EPA calculated risks for all
 combinations when the most sensitive
 parameters were set at high-end values
 and then used the highest "high-end"
 risk. In this way, EPA attempted to
 estimate "high-end" risks that were
 somewhere above the 90th percentila,
 i.e., the risks would be below this level
 for at least 90% of the population at
 risk. EPA also calculated "central
 tendency" risks, which correspond to
 the risk when all input parameters were
 set at their median value.
   Critical decisions for risk assessment
 include EPA's determination regarding
 which waste management scenarios to
 model and how to use the information
 on waste volumes and solvent
 concentrations disposed as modeling
 input. The Agency's modeling focused
 primarily on potential releases from
 wastes managed in aerated tanks, stored
 in open tanks, undergoing thermal
 treatment, and managed in surface
 impoundments. Modeling was based on
 the information EPA collected from
 facilities, including quantities of wastes
 managed. For each management
 scenario, EPA evaluated the full range of
 direct and indirect pathways through
 which the solvents could affect human
 health or the environment. Based on the
 physical and chemical properties of the
 constituents of concern and plausible
 management practices, certain routes  of
 exposure for some scenarios were not
 considered to pose threats and were not
 further evaluated.
  In general, solvent wastes fell  in
 several major categories. Wastewaters
 were typically diluted aqueous wastes
 that are managed in a biological
 treatment system (usually in tanks).,
 Nonwastewaters includes two
 subcategories. These include: (1) wastes
 with high levels of solvents or other
 organic chemicals, which were sent for
 thermal treatment in incinerators,
 industrial boilers, or fuel blenders, and
 (2) treatment residuals, such as
wastewater treatment sludges or
 incinerator ash, which contained
negligible levels of solvents.
  EPA modeled storage in an open tank
and thermal treatment for
nonwastewater spent solvent residuals
from use of all of the ten solvents. EPA
modeled wastewater treatment in

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64376    Federal Register/Vol. 63,  No. 223/Thursday, November 19, 1998/Rules and Regulations
aerated tanks for wastewater residuals
resulting from the use of acetonitrile, 2-
methoxyethanol, 2-ethoxyethanol
acetate, phenol, furfural, and cumene as
solvents.
  The surface impoundment scenario
was assessed for five of the solvents;
acetonitrile, phenol, cumene, furfural,
and methyl chloride.  For acetonitrile
and cumene, the headworks
concentrations (i.e., the concentrations
after the spent solvent was mixed with
other wastewaters at the headworks of
the wastewater treatment system)
potentially discharged to surface
impoundment were below the health-
based levels for these constituents, and
thus were not evaluated further. For
phenol, three wastewaters with spent
phenol were reported to be managed  in
surface impoundments that are part of a
wastewater treatment train. In two of
these cases, the phenol concentration
was below the drinking water health-
based level after mixing at the
headworks. prior to reaching the surface
Impoundment. In the third case the
stream had levels ranging above the
health-based level: however this level is
expected to be efficiently  treated by the
activated sludge, such that little phenol
would be available for release to
groundwater. For methyl chloride, EPA
modeled air releases from treatment in
a surface impoundment, but not the
groundwater pathway because the
impoundment was a permitted
hazardous waste management unit. (As
described below, the unit treating
methyl chloride wastes was unique due
to the highly specialized nature of this
solvent use). EPA modeled treatment in
a surface impoundment for furfural;
however, bounding analyses showed no
significant risks via air or groundwater
pathways. The solvent use of the
chemicals modeled in surface
impoundments are very specialized.
This means that they have properties
that only allow very particular solvent
uses in a very narrow set of
circumstances and only for some
industries, or even for only one. For
example, methyl chloride is a gas at
room temperature, which severely limits
its utility as a solvent. The only
significant solvent use for this chemical
is as a solvent in the polymerization of
butyl rubber, during which methyl
chloride is passed through aluminum
chloride to form and solubilize the
catalyst used. The chemical's special
ability to generate such a catalyst
solution is why it is used. Similarly, by
far the largest solvent uses of furfural
and phenol are in the extraction of a
high molecular weight oil (lubrication
oil) during petroleum refining; these
chemicals have very limited solvent
uses outside the petroleum industry.
Therefore, EPA has a high degree of
confidence that the concentrations of
chemicals in the streams flowing into
surface impoundments studied in this
listing determination  are representative
of the universe of such uses and
possible exposure scenarios.
  The landfill scenario was initially
assessed for acetonitrile, methyl
chloride, cumene, and cyclohexanol,
but not modeled for spent solvent
residuals from any of these solvents
because the concentrations in the wastes
were "trace" or "negligible." Further
general background for the risk
assessment is provided in the preamble
to the proposed rule (see 61 FR 42318).

III. Peer Review of Calculated
Toxicological Benchmarks

  Standard inhalation toxicological
benchmarks were not available to EPA
for four of the solvents when the Agency
was conducting the risk assessment for
the proposed rule. The Agency therefore
calculated values specifically for the
rule. EPA has labeled these toxicological
benchmarks "provisional RfCs" to
clearly differentiate them from the
Agency consensus values listed on IRIS.
During the comment period, EPA
solicited peer review of these calculated
risk values. The peer review reports and
the complete Agency response to the
reports are in the docket for this
rulemaking.
  In response to comments received in
the peer review reports, EPA adjusted
three of the provisional toxicological
benchmarks used for this risk
assessment. The changes are shown in
Table 1.
                       TABLE 1 .—CHANGES IN TOXICOLOGICAL BENCHMARKS FOR AIR PATHWAY
Solvent
Cyclohexanol 	
Phenol .. , 	 	 	
Isophorone 	
NOAEL1 (mg/m3)
0.06 	
.19 	
37(LOAEL)2 	
Previous provi-
sional toxi-
cological
benchmark
(mg/m3)
Q00006
Q019
0.0037
New provisional
toxicological
benchmark
(mg/m3)
0.00002
0.006
0.012
  1 No observed adverse effect level.
  2 Lowest observed adverse effect level.
  The new benchmarks for
cyclohexanol and phenol reflect
additional uncertainty factors to account
for insufficient toxicity databases. The
benchmark for isophorone reflects a
reduction in overall uncertainty factors
to reflect Agency guidance limiting such
factors to a total of 3,000. Full
documentation of the methodology for
developing these benchmarks is in the
docket for this rulemaking.
  In addition, the toxicological values
for cumene were changed on IRIS
during the comment period. The RfD
(for noncancer ingestion risks) was
changed from 0.04 mg/kg/day to 0.1 mg/
kg/day. The RfC (for noncancer
inhalation risks) was changed from
0.009 mg/m3 to 0.4 mg/m3. These
changes both reflect greater tolerance for
cumene than the previous benchmarks
and thus have no impact on EPA's
decision not to list wastes derived from
the use of this chemical as a solvent.
  The Agency has employed these
revised "provisional RfCs" for all the
updated risk assessments involving
these solvents for the final rule. In
addition, the Agency has re-estimated
risks assessed for the proposed rule
using these new benchmarks.
Documentation of these re-estimations
appears in the supplemental risk
assessment background document to
this final rule. The final risk estimates
for all the solvents are shown in Table
3 of this preamble.
  In all cases the changes to the
toxicological values do not have any
significant impact on EPA's risk results,
nor do the changes affect any listing
decisions. The solvent wastes for the
chemicals examined still do not pose
significant risks, and thus, these
analyses confirm the proposed decisions
not to list these  wastes.

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            Federal Register/Vol. 63, No. 223/Thursday, November  19,  1998/Rules and Regulations    64377
 IV. Summary of Response to Comments
 and Rationale for Final Rule
   The Agency is responding in this
 preamble to the most significant
 comments received in response to the
 document of August 14, 1996, 61 FR
 42318. Other comments received by the
 Agency are addressed in the document
 entitled Hazardous Waste Listing
 Determination: Spent Solvents,
 Response to Comments (hereafter
 known as Response to Comments
 Document) that is available  in the
 docket associated with this rulemaking.
   The Agency is responding to a variety
 of comments concerning data collection,
 methodology, risk assessment scenarios,
 and issues specific to each chemical in
 this listing determination. The
 responses, while touching many specific
 aspects of the listing determination
 effort, involve three major themes:
   • The Agency used a very thorough
 survey, which characterized the risks of
 the spent solvents. The Agency
 researched various potential
 applications of these chemicals as
 solvents and found that solvent uses are
 confined to a limited set of industrial
 applications. Data collected  from the
 questionnaires confirmed the general
 lack of wide solvent use, and are
 consistent with EPA's search of the
 literature. These findings allowed the
 Agency to consider the applicable waste
 generation and management practices,
 and define plausible management
 scenarios for use in evaluating potential
 risks associated with these solvent
 wastes.
   • Facilities use the solvents for
 specific purposes that vary by the
 desired process. Some of the solvents in
 this listing determination have different
 applications over certain industries (i.e.,
 acetonitrile). Even within one industry,
 the primary commonality among the
 processes is-the solvent constituent
 itself. Other solvents were used in very
 limited ways and their primary uses
 were highly specialized (e.g., furfural).
 However, even for solvents with
 specialized uses, other minor uses were
 typically reported for different
 industries and processes. The resulting
 potential variability in waste
 compositions led the Agency to focus its
 efforts on evaluating the solvent
 constituent itself. The Agency believes
 it has captured the risks that  arise from
 the solvents themselves, and that this is
 a reasonable approach to fulfilling its
 listing determination obligations.
  • Little to no benefit would accrue
from regulating these wastes  because
many are already regulated and treated
as hazardous wastes. These solvent
wastes, particularly nonwastewaters
 with a high organic content, are
 characteristically hazardous or mixed
 with other listed wastes, and are
 generally thermally treated. Other
 nonwastewaters, such as wastewater
 treatment sludges or filter media, do not
 contain measurable levels of the solvent
 constituents, and thus present no
 significant risks.

 A. Data Collection

 1. Representativeness of Industry
 Characterization
   One comment argues that EPA cannot
 fully characterize industry solvent
 management practices because the
 facilities that may be affected are too
 numerous to predict and specifically
 identify. Therefore, the Agency should
 project standard mismanagement
 scenarios in order to examine the full
 range of actual and potential waste
 management practices applicable to the
 wastes. This is the only way the Agency
 can discharge its mandate to protect
 human health and the environment.
  In response, EPA disagrees that it is
 not possible to predict and identify, as
 a practical matter, the facilities that may
 be affected. It is possible and
 appropriate to do so and EPA has, in
 fact, accomplished that purpose, as
 summarized below and explained more
 fully in the Response to Comments
 Document. The Agency outlined the
 general approach to the data collection
 process in the proposal (61 FR 42321-
 42322). To summarize, the Agency
 began collecting data on all 14
 chemicals involved in the listing
 determination (plus the seven in the
 Solvents Study) as a means of collecting
 background information on these
 chemicals. The Agency identified
 solvent uses through cross-referencing
 SIC codes in known and suspected
 process industries with data found in
 the TRI,  Office of Water facility lists,
 and many other data sources. The
 Agency used many different facility
 address lists to create a list of potential
 solvent-using facilities.
  The sources used by the Agency
 provide a comprehensive view of the
 types of uses of these chemicals as
 solvents and the quantities used. The
 Agency identified  industries using the
 14 chemicals as solvents by conducting
 literature searches including Chemical
 Abstracts, the Chemical Engineering
 Handbook, the Industrial Solvents
Handbook, and the SRI Chemical
 Economics Handbook. As today's
document and the associated
background documents explain, the
process was a logical, iterative, step-by-
step process. The chemicals in question
are not likely to be widely used as
 solvents (with the exception of
 acetonitrile and, to a more limited
 extent, 2-methoxyethanol, which have
 significant solvent uses in some
 industries), because they have
 properties that limit their use to specific
 situations, and are generally
 noncompetitive in price. In addition,
 the Agency's data collection
 methodology combined a
 comprehensive view not only of the
 chemical's solvent use, but also of
 nonsolvent uses to confirm use data.
 The specificity of applications for these
 solvents, while sometimes cutting
 across more than one industry, is still
 limited enough that the listing
 determination  could stay focused on the
 actual management scenarios found
 through questionnaires and site visits.
 The Agency is  confident that the waste
 management practice data found in this
 investigation are adequate for risk
 assessment modeling, and that using
 other modeling practices not found
 would only lead to using hypothetical
 waste data that do not represent any
 activities that resemble reality. To
 engage in this kind of hypothesis would
 be likely to result in forcing significant
 additional costs on the public with no
 incremental jisk reduction from
 regulating the wastes in question. The
 Agency notes that no commenter
 identified any specific solvent users of
 these chemicals not already found by
 the Agency. Also, the commenter could
 not suggest any alternative to the
 Agency's methodology other than a
 listing based on hypothetical
 uncertainties—an approach not justified
 by the data.
   The Agency sent almost 1,500
 preliminary questionnaires asking
 facilities how much of each chemical
 was used as a solvent in 1991 and 1992.
 The data showed that the Agency was
 successful in identifying many solvent
 users, although more than 900 facilities
 were eliminated from further
 consideration because they did not use
 any of the chemicals as a  solvent. The
 Agency was also able to eliminate
 another 400 facilities from consideration
 to receive the final questionnaires due
 to reporting errors, discontinued use, or
 reported  use of  small quantities of the
 solvents. The fact that the vast majority
 of facilities that received the
 preliminary questionnaire reported no
solvent use supports EPA's view that
many potential  solvent users, in fact, do
not use these chemicals this way. The
Agency found that reported uses of very
small quantities of the chemicals as
solvents were often inaccurate, but
facilities  reported these quantities to err
on the side of caution. The remaining

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64378    Federal Register/Vol. 63, No.  223/Thursday,  November 19,  1998/Rules and Regulations
156 facilities received a large, detailed
questionnaire requesting information on
solvent uses and waste generation and
management practices. The listing
determination is based on these data.
  The details of the data collection
effort also brought another point to the
Agency's attention. While other solvents
are used in countless industries and
facilities and would be difficult to
characterize, the particular set of
solvents in this listing determination
has much more limited applicability.
EPA's literature search found these
chemicals to have many and varied
"nonsolvent" uses. Data collected from
the questionnaires confirmed the
general lack of wide solvent use, as
discussed below.
  While reference sources  (e.g., SRI
Chemical Economics Handbook)
indicated many of these chemicals are
produced in fairly high quantities, these
references reported significant
quantities used.as solvent for only four
of the fourteen chemicals studied:
acetonitrile, 2-methoxyethanol, furfural,
and methyl chloride. This  is consistent
with what EPA found in its 3007 Survey
for these four chemicals. Furthermore,
as described in the Listing Background
Document and the proposed rule, the
solvent uses of furfural and methyl
chloride were limited to a single
specialized use in each case, and these
users were fully surveyed. Solvent use
quantities were not reported in
reference sources for the other ten
chemicals. Four of the ten were those
for which EPA also found no solvent
uses (benzyl chloride, epichlorohydrin,
ethylene dibromide, and p-
dichlorobenzene). For an additional
four, EPA's Survey found that the
amounts of the production quantities
used as a solvent were small compared
to total production (cumene-0.026%;
cyclohexanol-<0.1 %; 2-ethoxyethanol
acetate-1.2%; isophorone-1.7%); this is
also consistent with the lack of
significant quantities of solvent use
reported in reference sources.
  The remaining two chemicals are
special cases. The domestic production
of 2-methoxyethanol acetate is reported
to have ceased, and the small volume of
total solvent use found by EPA in its
Survey (1,673 kg/year) confirms the lack
of significant solvent use. EPA did find
Significant solvent use of the final
chemical, phenol, which was not
reported in most other reference
sources. However, nearly all (>99%) of
the solvent use quantity found in the
Survey was from one facility that
produces phenol for its own captive use.
This "native" phenol is produced as a
byproduct of other processes, and
would not be reported in production or
use data in reference sources. Leaving
out this volume from one facility, EPA's
Survey shows that the fraction of phenol
production that is used as a solvent is
low (<0.2%), which is consistent with
the lack of any significant solvent use
quantities reported in reference sources.
In any case, the vast majority of phenol
solvent use reported in the 3007 Survey
was a very specialized use; the
petroleum industry uses phenol to
extract lube oil from residual oil. EPA
surveyed all petroleum refiners in its
Survey; thus EPA is confident the
Survey captured all major solvent users
for this chemical.
  The Agency disagrees that it should
project standard mismanagement
scenarios not indicated by the data,
because the rationales for selection of a
particular set of plausible management
scenarios are specific to each solvent.
Based on the general rationale just
discussed and the data for each of the
chemicals as given in detailed
discussion in the Response to
Comments Document for each of the
chemicals, the Agency has confidence
in the data set as the best available effort
to assess the chemical use universe and
actual waste generation and
management scenarios. Merely
developing hypothetical waste
generation and management scenarios,
as suggested by the comment, has no
sound basis in fact. This would lead to
the danger of over regulating risks that
do not exist and siphoning off scarce
resources to deal with those non-risks,
rather than risks that may be more
worthy of the public's attention.
   For these solvents, the Agency has no
reason to project management scenarios
beyond what was found through
questionnaires and site visits. The
Agency found the vast majority of
wastes managed in tanks and
incinerators. Where a waste was
managed in a surface impoundment, the
Agency performed that modeling under
high-end exposure assumptions. The
Background Document to the proposal
and the Response to Comments
Document both present more detailed
assessments of how each individual
chemical is used, what wastes are
generated, and what management
scenarios were selected. For example,
no management scenarios were selected
for p-dichlorobenzene, epichlorohydrin,
ethylene dibromide, and benzyl
chloride because none of these
chemicals are used as solvents. For most
other chemicals, the uses are extremely
limited and specific. See the sections
devoted to the individual chemicals for
specific rationales, and the discussion of
management scenarios in section IV.B.4.
  Below, EPA responds to the specific
issues raised in comments that the
Agency's survey was inadequate to
characterize the solvent uses and
mismanagement scenarios.
  One commenter pointed out that EPA
surveyed only a small percentage of
facilities within very few SIC codes. The
commenter stated that for several
solvents, the quantity of sectors
potentially affected outnumbers the
quantity of facilities forming the basis
for EPA's plausible mismanagement
conclusions. As an example, the
commenter stated that for 2-
methoxyethanol acetate, EPA identified
seven industrial sectors potentially
affected by this chemical, but sent only
the questionnaire to three facilities
using the solvent.
  The Agency disagrees with this
comment. As previously mentioned,
this listing determination covers 14
chemicals used as solvents. In order for
the Agency to determine the universe of
facilities potentially affected by this
listing determination, it sent out
preliminary information surveys to
obtain basic solvent use information.
The Agency sent this survey to nearly
1500 facilities based on an evaluation of
chemical usage. Given this large
universe of facilities and the potential to
obtain useful information on solvent use
in this mailing, the Agency also decided
to include in  this preliminary
questionnaire questions concerning
seven other chemicals (in addition to
the 14 already included in this listing
determination) which it was also
investigating  under a Solvent Study
mandated by the court.
  The prequestionnaires showed that
about 600 facilities reported any
possible use of one or more of the
chemicals as  solvents. The Agency
conducted further evaluations and
screening and identified 156 facilities to
which it sent the more detailed "full"
questionnaire concerning the use of the
21 chemicals as solvents (14 for this
listing determination and 7 for a
separate Solvents Study). Thus, only
about 10% of the facilities that were
sent preliminary questionnaires used
significant amounts of these chemicals
as solvents. As described in today's
document in  response to other
comments, this screening removed
facilities that did not use the chemical
as a solvent (as defined by EPA), and
small volume users. For a more detailed
description of this screening and
evaluation see, please refer to section
III.A in  the Response to Comment
Document for'this rulemaking.
  The results of this final questionnaire
showed that 4 out of the 14 chemicals
in this listing determination were not

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            Federal  Register / Vol. 63, No. 223/Thursday, November 19,  1998/Rules and Regulations     64379
 used as solvents and that 10 of the 14
 chemicals were used a solvents to
 varying degrees. The industry sectors
 listed by SIC code by the commenter are
 ones which typically do not use any of
 the 14 chemicals as solvents and, thus,
 did not yield data to be considered in
 evaluating plausible management
 scenarios. Further, as discussed earlier
 in this section, all other indications
 from the Agency's survey show that the
 amounts of solvent use  EPA found were
 generally comparable to the solvent use
 found in other references. The volume
 of solvent use found by the Agency is
 also consistent with what the Agency
 knows about the likely technical
 usefulness of these chemicals as
 solvents. A limited set of industries
 exists in which these chemicals are used
 as solvents, as discovered through
 standard reference sources.
   The commenter presented a plethora
 of small companies on the SIC code list
 that operate on lower margins. The
 Agency believes that these companies
 are not likely to use these higher cost
 chemicals for generic solvent use
 processes. The Agency believes that if
 any of these chemicals had been used as
 solvents in other industries, as the
 commenter postulates, the Agency
 would have found this information
 during its data collection. The facilities
 surveyed by the Agency share many
 processes with the large number of
 smaller facilities in the lists presented
 by the commenters  (equipment
 cleaning, electroplating, etc.). However,
 the chemicals at issue are rarely,  if ever,
 used as solvents in those processes in
 the facilities found by the Agency.
   Also, the Agency recognizes that the
 commenter cites a greater number of
 facilities within each SIC code than the
 number to which EPA has sent
 questionnaires. These facility numbers
 are obtained from a data base (Dun &
 Bradstreet) that is not linked to
 chemical use. Many of the addresses
 represent corporate  headquarters, not
 facilities that use  or generate hazardous
 waste, and a single facility may have
 more than one Dun & Bradstreet
 number. Therefore, EPA believes that
 the number of facilities reported within
 each SIC code based on this data is
 exaggerated.
  The commenter cites 2-
 methoxyethanol acetate and methyl
 chloride as examples, stating that "EPA
 identified seven industrial sectors
potentially using 2-MEA, but only three
facilities using the solvent received the
final questionnaire." As presented in
the background document, 14 facilities
received the full questionnaire based on
their response to the preliminary
questionnaire. However,  based on their
 response to the full Survey, 11 of these
 14 facilities discontinued use of 2-MEA
 or did not use it in a ma'hner that met
 the regulatory definition of solvent use.
 Only two industries reported using 2-
 MEA in 1994 that met the definition of
 solvent use. The commenter further
 states "In the case of methyl chloride,
 EPA identified eight SIC codes
 potentially using the solvent, while only
 seven facilities received the final
 questionnaire." As presented in the
 background document, 32 facilities
 received the full questionnaire based on
 their response to the preliminary
 questionnaire. However, based on their
 response to the preliminary
 questionnaire, 24 facilities were TSDs,
 and as a result the chemical
 consumption reported could not be
 linked to solvent use. Other facilities
 did no't use methyl chloride in a manner
 that met the definition of solvent use, or
 used extremely small volumes (less than
 1  kg) that generated wastes with no
 methyl chloride. Thus, this left only
 four facilities that reported solvent use
 of methyl chloride in two industries,
 and essentially all of this use was in the
 synthetic rubber manufacturing.
   One commenter stated that EPA chose
 to review chemical abstracts for only a
 four-year period, and for other solvents
 limited the search to a 10-year period.
 Therefore, older uses of the solvents
 would not have been identified through
 the literature search. The commenter
 also states that newer or less studied
 solvent uses would not appear in the
 public literature. The commenter
 disagrees with the Agency's assertion
 that few, if any, solvent uses were
 missed using this method.
   In response, the Agency does not
 believe that searching Chemical
 Abstracts for an unlimited time period
 for all 14 solvents is justified. If a
 process was developed more than ten
 years ago and  is still in use today, it
 would appear in more recent Chemical
 Abstracts or be reflected in alternative
 data sources, such as Effluent
 Limitations Guidelines or the SRI
 Chemical Engineering Handbook.
 Furthermore, the further back the search
 is  conducted, the more unlikely that the
 use identified  will still be employed
 today. Newer solvent uses, if confined
 to  small scale laboratory use, would not
 change the solvent use universe
 significantly and would be reported as
 laboratory waste (and managed
 accordingly, most likely as a hazardous
 waste because spent solvents exhibit a
 Characteristic or contain listed wastes).
 Once such a process enters large-scale
 commercial use, reporting generally
appears on some standard database or
literature source that the Agency would
 find. The probability that a solvent use
 would, in one year, not exist and then
 appear in large scale is extremely low.
 Small volume solvent uses of these
 chemicals are not critical to EPA's
 evaluation, because any risks from
 larger volumes usage (and
 corresponding larger loadings in wastes)
 are likely to be of greater concern. Most
 of the companies that would conduct
 the types of research and development
 to find new uses are generally reporters
 to databases like the TRI, and as such,
 would report any significant uses of
 these solvents.
   The commenter also stated that some
 chemicals, such as cyclohexanol,
 furfural, and isophorone, are not
 reported  under TRI. For the remaining
 solvents, TRI reporting is not required
 when chemicals are "otherwise used" in
 quantities of 10,000 pounds or less
 (equivalent to 4,540 kg or less). The
 commenter argued that substantial
 quantities of the solvents can be used
 and not reported under TRI.
   In response, in cases of the three
 chemicals for which the TRI data  base
 was inadequate, the Agency relied on
 other sources more heavily. In fact, the
 TRI was only one source for all
 chemicals in the listing determination,
 even those covered by TRI. Because the
 Agency was aware that these chemicals
 were not required to be reported
 pursuant  to TRI at the time of the
 solvent use industry characterization,
 the Agency relied on additional sources
 cited in the Listing Background
 Document. Through literature searches,
 potential solvent  uses were identified in
 several SIC codes for cyclohexanol,
 furfural and isophorone.
   Moreover, since the questionnaire
 data were collected, the Agency added
 cyclohexanol to the TRI. Analysis of TRI
 chemical  use data on cyclohexanol
 confirms the Agency's literature search
 and determination of the universe of
 users of this chemical as a solvent.
 While 24 facilities reported
 cyclohexanol manufacturing processes
 in the TRI, only one facility reported the
 "otherwise use" category of
 cyclohexanol that could potentially be
 solvent use: Thus, the TRI data show
 that the Agency might have sent out
 only one additional preliminary
 questionnaire  (EPA received 37
 responses to preliminary questionnaires
 for cyclohexanol). Further investigation
 by EPA revealed that cyclohexanol was
 not used as a solvent at this one site.
This new information substantiates
 EPA's original findings that there are no
other large users of cyclohexanol as a
solvent. See section III of the Response
to  Comments Document in the docket
for details of the new TRI information.

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64380    Federal Register/Vol. 63, No.  223/Thursday,  November 19,  1998/Rules  and Regulations
  The commenter argued that many of
the solvent uses EPA did identify
involve extremely high concentrations
of the chemicals, up to and including
pure solvent. These pure solvent uses
can generate wastes in quantities 100
times larger with concentrations of 1%,
still significantly in excess of
concentrations that may pose a
substantial risk to human health or the
environment.
  The Agency disagrees with the
commenter that the risks of concern
were not analyzed. In fact, the Agency's
modeling considered environmental
loadings of these chemicals resulting
from solvent uses ranging from 100
percent to the part-per-million (ppm)
level. The Agency evaluated  potential
releases of high percentage solvent uses
that lead to greater loadings than would
result from a one percent level in the
waste. Modeling of these chemical
releases under high end exposure
conditions did not result in risks of
concern.
  In response to the commenter's
concerns that small volume users might
generate wastes of concern, perhaps due
to different management practices, the
Agency examined the data in hand from
the Survey for such users. Facilities that
received Surveys due to significant use
of some solvents (> 1,200 kg/yr), also
used other solvents in lower volumes in
some cases. Thus, the Agency has data
on wastes from facilities that used small
volumes of solvents, (see Listing
Background Document, Appendix I).
EPA reviewed the management
practices for wastes generated by these
smaller volume uses to see if any
differences were evident. For all 10
solvents, EPA found a total of 73 wastes
that were generated from solvent uses
below 1,200 kg. The Survey data show
that these  were managed in ways that
were very similar to practices reported
for larger volume uses. Of these 73
wastes, 69 were incinerated or
otherwise thermally treated (nearly all
were classified as hazardous  because
they exhibited a hazardous
Characteristic, or due to the presence of
other listed hazardous waste), three
wastewaters were treated in tanks, and
one wastewater was treated in a surface
impoundment (the chemical  in the
impoundment, acetonitrile, was
evaluated through modeling).
Furthermore, 67 of the 73 wastes
reflected solvent use at concentrations
of 50-100%, i.e., many of these wastes
were generated from use of solvents at
high concentration. None of these
wastes from small volume users present
any special risk, because risk analyses
using larger loadings going to these
management practices found no
significant risks. Therefore, the existing
data support EPA's belief that wastes
from small volume users are not of any
special concern. Furthermore, these
wastes are nearly all handled as
hazardous, which is also consistent with
the general pattern found for other
larger volume wastes.
  Two commenters stated that they
agreed with EPA's decision to limit the
solvents listing investigation to facilities
that use a combined total of 1,200
kilograms or more per year of all
chemicals of concern used as solvents
because the commenters feel that this
level represents a  reasonable
characterization of the universe of
solvent users. One of these commenters
requested clarification to ensure this
approach would not be misconstrued by
hazardous waste generators when
determining their generator category. In
response, the Agency is confirming that
the cutoff categories used by the Agency
in this listing determination are not to
be construed by any actual or potential
hazardous waste generators to be a
means of determining waste generator
categories. Furthermore, EPA did
consider  solvent uses below the 1,200
kg threshold as noted above, however,
the Agency found that such small
quantity use is highly unlikely to
present risks of concern when compared
to the risks from larger users.
  However, another commenter stated
that EPA's rationale for deleting
facilities  using 1,200 kg or less of
solvent in 1992 was that only large
quantity solvent users could be
expected to have treatment, storage, and
disposal  (TSD) units on-site, and that
many of the solvent uses are peculiar to
large companies. The commenter stated
that this limitation in the data collection
introduces bias against solvent
generators relying upon commercial
services,  including offsite nonhazardous
landfills, for their waste management
needs. The commenter then argued that
the Agency cannot assume offsite
disposal  in a nonhazardous waste
landfill is rarely practiced when EPA
intentionally excluded those facilities
most likely to use such facilities by not
surveying smaller volume users.
  The reasoning cited by the commenter
is taken out of context and does not
reflect EPA's rationale. EPA did not
decide to eliminate small volume users
because they would not have on-site
treatment capabilities. Rather, EPA
determined that the burden of
completing a complex, 100-plus page
questionnaire would not be
commensurate with the value of the
information EPA would receive. EPA
would not gain useful information from
small users because many of these
facilities, if they use these chemicals as
solvents at all, would present low risks
compared to larger solvent users.
Furthermore, as noted above, EPA did,
in fact, capture small users of solvents
in the full Survey, and found no special
management or risk concerns that were
not reflected in  it evaluation of larger
solvent users.
  Facilities are likely to use on-site as
well as off-site waste management
practices, and sometimes a combination
of the two. This is evidenced in
responses to the 3007 Survey, wherein
respondents indicated that both on-site
and off-site practices were employed.
The 3007 Survey has captured
numerous facilities that use commercial
services. Based on the results of the
Survey, 62 percent of the wastestreams
are managed in  commercial offsite
treatment or disposal units. As such, the
Agency does not believe there is any
significant bias in its Survey.
  In addition, EPA points out that the
vast majority of small solvent users
eliminated by EPA reported using
amounts well below the  1,200 kg
threshold. In fact more than 90% of
those eliminated reported used less than
120 kg total for all of the solvents
studied. EPA found that  uses of such
small volumes typically were reported
for laboratory uses, are difficult to
verify, and may be reported as solvent
use if laboratory uses are not known.
The 1,200 kg/yr cutoff is an appropriate
surrogate for identifying facilities that
may potentially generate large amounts
of hazardous waste or waste with high
solvent loadings. EPA believes the
facilities with larger solvent uses would
be most likely to provide useful data
through the questionnaire, i.e.,  data
based on verifiable solvent use  that
could then be used in developing risk
assessments.
  One commenter argued that solvent
use fluctuates from year to year, thus
uses below 1,200 kg could  increase
dramatically in  the future due to process
changes, increases in production, or
solvent substitutions. The commenter
went on to state that use volumes for
some solvents reported in the final
questionnaire for 1993 were higher than
the rates reported for the same facilities
in the preliminary questionnaire for the
prior year. The commenter stated that
EPA fails to appreciate the consequence
of these fluctuations and substantial
changes can be expected from year to
year, e.g., a facility using less than 1,200
kg of solvent one year may use  more
than that amount the next year. The
commenter concludes that EPA lacks an
objective basis for simply assuming the
data it collected is fully dispositive with

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            Federal Register/Vol.  63,  No. 223/Thursday, November  19,  1998/Rules and Regulations    64381
 respect to future solvent uses and
 management practices.
   EPA believes that the data collected
 provides a reasonable bases for
 decision-making. The purpose of the
 preliminary questionnaire was to
 capture what occurs at the facilities
 surveyed during a typical year. As was
 expected, some facilities' solvent use
 consumption decreased between the
 two years and other facilities' solvent
 consumption increased between the two
 years. The Agency does not expect
 solvent consumptions to be identical
 from year-to-year, but has no data to
 indicate that 1993 is an atypical year.
 Even if the specific facilities meeting the
 cutoff varied from year to year, EPA
 believes the data gathered from facilities
 studied provide a representative
 database. The Agency used the most
 recent data when determining the 1,200
 kg cutoff for those facilities receiving
 the full questionnaire.
   EPA considered whether or not
 solvent management practices were
 likely to change in the future from those
 reported in the 3007 Survey. The
 Agency determined that there was no
 reason  to believe that they would,
 regardless of the volume fluctuation. In
 the case of wastewaters, EPA has no
 reason  to believe that a facility would
 convert from a tank-based system to a
 surface impoundment given the capital
 investment and liability issues
 associated with land-based treatment,
 particularly when facilities do not have
 the physical space for a surface
 impoundment or have closed surface
 impoundments in favor of tank-based
 systems. For nonwastewaters, EPA has
 no reason to believe that a facility
 would switch from the thermal
 treatment of high organic wastes to
 disposal in a nonhazardous landfill due
 to the BTU value and the liability issues
 associated with land-based disposal.
  The Agency cannot accurately predict
 with specificity future uses of the
 fourteen chemicals, nor is it reasonable
 for EPA to regulate solvent waste based
 on some purely hypothetical future use.
 While the solvent consumption may
 change  over time for some facilities,
 such fluctuations are unlikely to
 significantly affect EPA's current risk
 conclusions for several reasons. First, in
 its risk analyses EPA used high-end or
 maximum solvent loadings to project
 potential risks. Thus, EPA's evaluation
 is not likely to change due to some
 volume use fluctuations. In addition, for
 most of these solvents (and specifically
for three noted by the commenter,
acetonitrile, 2-methoxyethanol acetate,
and isophorone), the vast majority of
wastes are regulated as hazardous due to
the hazardous waste characteristics (see
 40 CFR 261.20-261-.24) or mixing with
 other listed wastes. Thus, any increase
 in volume use would result perhaps in
 somewhat higher solvent quantities
 reaching wastes that would be already
 regulated and thus unlikely to pose
 significant risk. Therefore, while EPA
 agrees that its Survey is more-or-less a
 "snapshot" of waste generation data, the
 Agency continues to believe that such
 an approach has yielded data that are
 representative, and is a reasonable way
 to assess potential risks.
   The commenter also stated that EPA
 excluded any laboratory uses of the
 solvents from the universe of facilities
 receiving the preliminary questionnaire,
 notwithstanding the Agency's
 observation that "lab use" of chemicals
 was not restricted to small volumes.
   The Agency did not exclude
 laboratory uses of solvent from the
 universe  of facilities. The Agency was
 precluded from sending a 3007 Survey
 to all laboratories due to the sheer
 number of labs that exist in the United
 States, approximately 183,000 according
 to an estimate by EPA. (For details
 please refer to the Response to
 Comments Document). Many of these
 laboratories are small, comprising
 research labs (12,500), medical
 laboratories (22,700), and university
 labs (108,000), as well as small
 analytical labs (40,000). The resources
 necessary to complete a RCRA 3007
 questionnaire would be beyond the
 means of many of these small
 businesses as organizations.
 Nonetheless, the Agency captured the
 solvent uses and management practices
 of numerous (32) captive on-site
 laboratories of facilities who received
 the 3007 Survey. In doing so, the
 Agency captured large research, QA/QC,
 and analytical laboratories that operate
 at the same or larger scale as the small
 labs not surveyed. Approximately 38%
 of the laboratories captured were small
 laboratories (i.e., using <1,200 kg of
 solvent use).
   The Agency found that in industrial
 facilities,  the proportion of laboratory
 use of a solvent compared with the
 chemical process use is about 1% or
 less. After consulting with the American
 Chemical Society, college and
 university hazardous waste managers,
 standard references, and OSHA
 guidelines, the Agency determined that
 laboratory wastes are managed as
 hazardous because they are usually
 mixed with other hazardous wastes,
 often with acutely hazardous wastes. In
 addition, with the exception of
 acetonitrile (which has specialized uses
 in laboratories as a solvent for high
pressure liquid chromatography, or
HPLC), the reported use of any of these
 chemicals is suspect, and is attributable
 to facilities reporting "solvent use" in
 the questionnaires as a precautionary
 measure. Few of the chemicals under
 examination are likely to find extensive
 use as solvents in the laboratory. For
 example, very few of the standard
 laboratory test methods specified by
 EPA call for use of these chemicals as
 solvents. For a complete summary of the
 laboratory use of solvents please refer to
 the Response to Comments Document.
 2. Engineering Site Visit Reports
   One commenter stated that the
 engineering site visits were superficial
 and did not encompass a thorough
 review of waste management, solvent
 waste characteristics, and potential
 environmental releases or damage from
 waste handling. The commenter
 acknowledged that EPA's objective for
 the site visits was simply to determine
 if a facility should be sent a full
 questionnaire, and to educate the
 facility on the solvent listing process,
 but stated that this seems like a waste
 of effort, given that more valuable
 information could have been obtained
 from the site visits regarding waste
 properties, handling and environmental
 damages.
   The commenter also noted that none
 of the visits involved any sampling
 efforts. No analytical or characterization
 data are presented on the concentrations
 of solvent constituents in the waste
 streams observed at the industrial sites
 visited. The visits were typically two
 hours, with anywhere from 0-60
 minutes spent actually touring the
 facility. One site visit was conducted
 from a tour van and was strictly a
 "windshield audit," and two were
 strictly conference room audits. The
 reports did not investigate, evaluate, or
 address any historical spills, releases to
 groundwater or surface water, or any
 other environmental damage from use of
 the solvent or handling of the wastes.
   These comments misconstrue the
 reasons EPA conducted the site visits
 and the information that could
 practically be developed from them. The
 purpose of the site visits was to
 familiarize the Agency with the
 multitude of processes and industries
 potentially subject to the investigation
 through "first person" experience rather
 than "textbook" learning. The Agency
 disagrees that the Engineering Site
 Visits were superficial given their
 purpose of site familiarity, not data
collection. The Agency points the
commenter to the engineering site visits
reports that each state EPA's objectives
in undertaking the site visit—of which
those cited by the commenter are but
two. The site visits were performed to

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64382    Federal Register/Vol. 63, No.  223/Thursday,  November  19,  1998/Rules and Regulations
obtain a first hand understanding of
solvent utilization and also to develop
a working relationship with the
industries. Moreover, the site visits
served as an outreach mechanism for
EPA to interact with industry and
inform potentially affected industries of
the investigation. Site visits afforded
EPA staff an opportunity to become
familiar with processes used in specific
industries, field test the questionnaire,
and assess ongoing pollution prevention
activities.
  EPA obtained the "valuable
Information" cited by the commenter in
a more comprehensive way through the
questionnaires. EPA collected data on
waste properties and management
practices through the 3007 Survey,
which contains detailed, site-specific
information from 156 facilities. It would
not be practical for EPA to visit all sites
to gather detailed information on
solvent use. Therefore. EPA's reliance
on the 3007 Survey is eminently
reasonable for collecting information on
waste characterization data, release, and
waste management practices. Visits
conducted following the receipt of
RCRA 3007 Questionnaires helped EPA
to better understand the type of
processes  used in target industries and
the data provided by respondents, and
also provided confirmation of the data
provided.  The Agency was able to focus
on larger scale users and specific
processes  up-close, based on the
information reported in the 3007
Survey.
  As discussed in detail in the Response
to Comments Document, tours of the
facilities lasted as little as 1.5 hours and
as much as 3.5 hours, with a minimum
of 30 minutes and a maximum of more
than 2 hours spent on tour and/or on the
plant floor. Information related to spills,
releases and other environmental
damage was requested in the 3007
questionnaire and collection of this type
of information was not the focus of
these visits. The Agency takes issue
with the commenter's characterization
of the visits as "windshield audits."
None of the site visits were mere tours
from a van. The Agency personnel
witnessed many operations on a site and
were able to walk around the facility.
The commenter also mischaracterized
several other details of individual site
visit reports. The Agency has corrected
these misconceptions in the Response to
Comments document and provided
clarification to clear up any confusion,
as necessary. For more detail on the
sampling  issue, please refer to section
IV.B.2 of today's document.
B. Methodology
1. Definition of "Solvent"
  One commenter objected to the
Agency's characterization of solvent use
as too limiting, stating that solvents
contained in paints, coatings, dyes,
fuels, etc. are still mobilizing agents,
and that they unleash the same
environmental impact when these
products are spilled or released. The
commenter also points out that being
able to solubilize or mobilize other
constituents in a formulation still meets
the Agency's definition of solvent use.
  The Agency disagrees, and notes a
long-standing policy of treating these
cases differently. The discussion of the
scope of the solvent listings and the
applicable definitions appears in section
IB, above. As noted there, process
wastes where solvents were used as
reactants or ingredients in the
formulation of commercial chemical
products are not covered by the listing.
The products themselves also are not
covered. The commercial formulations
in which solvents are often ingredients
are generally products that are not
wastes under RCRA. Where  these
products are not in some way already
regulated, the Agency could examine
these materials if they become wastes
and if deemed necessary. However, with
a backlog of listing determinations to
complete under court-ordered
deadlines, the Agency has focused its
current efforts on those determinations
required by law. The Agency is under
direction from Congress to consider
listing wastes from "solvents" and that
direction has been incorporated into the
Consent Decree. Thus, the Agency has
focused its resources on the rather
narrow set of risks described in this
Federal Register document and the
rulemaking record for this decision.

2. Lack of Sampling and Analysis
  Two commenters objected that EPA
performed no sampling and analysis of
these waste streams. One commenter
stated it is impossible for EPA to come
to any listing determination without
some independent sampling and
characterization of these wastes. Useful
characterization data could  have been
obtained by sampling wastes from a
subset of the 156 respondents
representative of all the SIC codes using
the wastes, according to this
commenter.
  EPA does not agree that it would
obtain useful information from
independent sampling of the solvent
wastes. The solvents listing
determination covers a number of
industries using different solvents for
different purposes and in different
ways. The greatest challenge would be
in collecting a sufficient number of
samples to characterize each of these
uses. Assuming that EPA were to
sample all 10 solvents, obtain both a
wastewater and a nonwastewater
sample, and gather samples from the
industries using the  solvents (at an
estimate of three industries on average
per solvent), the baseline number of
samples required would be 60. In
addition to baseline  samples, to conduct
a valid sampling exercise the Agency
also would need to sample for
variability, that is, the Agency would
take samples at several locations within
a single facility and  would take samples
at several facilities within an industry
group using the same solvent. Assuming
that an additional two samples are taken
within the same facility, and then an
additional two facilities are visited, the
total number of required samples
reaches 540. This number still might not
allow EPA to fully characterize solvent
wastes. Thus, the Agency would be
spending scarce resources on a massive
sampling effort, when the data need
could be more efficiently obtained by
methods other than  independent
sampling. While EPA could attempt a
more limited sampling approach, the
result would not be  likely to provide a
sound basis for  making  listing decisions.
  By definition, the  concentration of the
solvent must be relatively high before
use, and this would  allow use of mass
loadings in calculating maximum waste
levels, as needed. The Agency felt that
it could rely on the questionnaire data,
and no information  has been submitted
in comments to show that sampling and
analysis was needed to  confirm the
concentrations in the solvent wastes
reported. The facilities provided ranges
of concentration where  concentrations
within a waste stream varied. When
data were reported as ranges, the
Agency used the high end of
concentration ranges as a conservative
approach in its  risk  assessment.
  The Agency does  not have reason to
believe that the solvent concentrations
reported are underestimated. In many
instances copies of laboratory data
showing the solvent concentration (s) in
a sampled residual were provided with
the respondents' 3007 survey. The
reported data seem reasonable and
correspond with observations of
residual streams during Engineering Site-
Visits. The solvent concentrations and
residual volumes were further
substantiated through mass balances
performed on the solvent use processes
by reviewing the 3007 survey responses
(see section III.B of the Response to
Comments Document).  EPA evaluated
the data contained in the 3007 Survey

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           Federal Register/Vol.  63, No. 223/Thursday, November 19, 1998/Rules and  Regulations    64383
 responses for any inconsistencies or
 missing residuals. If any inconsistencies
 or missing residuals were found, a
 follow up phone call was made to the
 appropriate facility for additional
 information. Where applicable, this
 additional information can be found in
 the docket along with the 3007 Survey
 Responses. Therefore, the Agency feels
 comfortable that it can rely on the
 reported data to adequately characterize
 risk.
  EPA has used 3007 Survey data
 extensively in the past in making listing
 determinations. In this case, each survey
 was signed by the responsible party to
 indicate that the information reported is
 accurate. The Agency does not have
 reason to believe that the facilities
 would falsify or omit any of their data
 in light of the substantial penalties  for
 submitting false information. In
 instances where concentrations were
 unclear or unreported, telephone
 contact was made with the facility.
  Two commenters stated that EPA is
 required to consider the presence of any
 hazardous constituents, not just the
 solvent itself, because other hazardous
 constituents may be present in the waste
 due to impurities, other chemicals used
 in the same processes or managed in the
 same equipment as the solvents, and
 chemical reactions occurring in such
 processes or equipment.
  EPA does not agree that the Agency is
 required to consider other constituents
 present in the wastes examined. Indeed,
 due to the extreme variability of these
 other constituents in the solvent wastes
 across industries, EPA would
 undoubtedly find it impossible to
 categorize these wastes under 40  CFR
 261.11 (b) if it considered the other
 constituents. The solvent uses found for
 acetonitrile illustrate this problem
 graphically. Acetonitrile is used as a
 solvent in various industries, including
 Pharmaceuticals, petrochemicals,
 photographic chemicals, and other
 chemical manufacturers (see the Listing
 Background Document, section 4.0). The
 actual uses of acetonitrile also are
 variable, and include uses as a reaction
 medium for the synthesis of numerous
 different chemicals, and as
 chromatographic eluent for analytical or
 preparative separation of various
 chemicals from different impurities.
 Wastes resulting from such widely
varying processes across different
 industries cannot be expected to have
 consistent waste constituents, except for
the solvent itself.
  As the commenter pointed out, other
constituents could originate from
various sources in the use of a solvent.
Thus, other constituents are dependent
on other solvents used, the specific
 solvent use, other processes carried out
 at a facility, other wastes that may be
 generated .from other processes onsite,
 etc. Because of the wide variability in
 waste constituents that might arise in
 wastes from use of the solvents, the
 Agency focused on the solvent chemical
 itself. Other constituents may vary
 widely for different industries and
 solvent uses; thus, the Agency believes
 the only practical approach to
 evaluating such wastes for potential
 listing is to consider the risk posed by
 the solvent chemicals under
 examination.
  The language in the existing F-listed
 solvents illustrates EPA's special
 concern with the solvents themselves in
 defining the scope of the listings; the
 listings are applicable only to wastes
 derived from the use of the solvents at
 levels of ten percent or more. In the case
 of the current solvents rulemaking, the
 Agency evaluated the common set of
 chemicals, i.e. the 14 solvents of
 concern. The Agency's assessment of
 these 14 solvents shows no risk to
 human health or the environment from
 these wastes, as discussed in detail
 elsewhere in this document.
 3. Consistency of Methodology With
 Other Listing Determinations
  One commenter asserted that,
 contrary to EPA's claim, the listing
 determinations in today's rule were
 based on scenarios that are different
 from those EPA used in both the
 proposed Dyes and Pigments listing
 determination (59 FR 66072, Dec. 22,
 1994) and the proposed Petroleum
 Refining Process waste listing
 determination (60 FR 57747, Nov. 20,
 1995). The commenter stated that in the
 Dyes and Pigments proposal, EPA used
 plausible mismanagement scenarios of
 disposal in unlined municipal  landfills
 and on-site monofills, in addition to
 other plausible scenarios (wastewater
 treatment tanks, industrial boilers). The
 commenter stated that in the'Petroleum
 Refining Waste determination EPA also
 considered plausible mismanagement
 scenarios, including disposal in on-site
 and off-site Subtitle D landfills. The
 commenter argued that EPA did not
 follow the policy used in the Dyes and
 Pigments and Petroleum Refining rules
 in the proposed solvent listing  because
 EPA did not consider mismanagement
 scenarios that reasonably could be
 employed,  particularly land disposal in
 unlined landfills. The commenter stated
 that there is nothing that prevents a
 solvent waste generator from land
 disposing the solvent waste, and
substantial evidence of land disposal
 practices was found in the docket to the
 proposed solvent rule.
   In response, EPA disagrees that the
 methods for determining plausible
 management scenarios in this rule is
 inconsistent with either the proposed
 Dyes and Pigments listing or the
 Petroleum listing. In both cases, EPA
 used appropriate evidence to evaluate
 current conditions and to project
 plausible future scenarios. The Agency
 does not presume unlikely worst cases
 or hypothesize scenarios that are not.
 likely in the interests of avoiding listing
 decisions that would not result  in
 incremental benefits to public health or
 the environment. See Dithiocarbamate
 TaskForcev. EPA, 98 F.3d 1394, 1401
 (D.C. Cir. 1996).
   With respect to the Dyes and
 Pigments proposal, management in
 unlined municipal landfills and on-site
 monofills was reported in the 3007
 Survey for certain wastes. EPA found
 that nearly all dye and pigment  waste
 sludges/solids studied had, in fact, been
 disposed in unlined municipal landfills.
 Thus, the Agency determined that
 placement in an unlined landfill was
 plausible for most dye and pigment
 wastestreams.
   However, EPA did not consider
 disposal in landfills plausible for all
 Dyes and Pigment wastes, and
 considered the specific facts for each
 waste. For example, EPA proposed not
 to list one category of waste, wastewater
 treatment sludges from the production
 of triarlymethane pigments using
 aniline as a  feedstock, despite risks that
 might arise if the waste were send to a
 landfill. For this waste category, EPA
 determined  a landfill was not plausible
 management (see 59 FR 66096).  This
 was because the current management
 practice was blending with fuel  for
 combustion, and EPA decided that the
 high organic content and fuel value of
 the waste made it implausible that
 landfill disposal would occur. This is
 entirely consistent with EPA's approach
 in today's rule for a similar waste
 derived from use of acetonitrile  as a
 solvent. As described in the specific
 section on acetonitrile (section IV.D3),
 EPA does not view risks that might arise
 from landfill disposal as significant
 because such disposal is unlikely given
 the current practice of fuel blending and
 the confirmed fuel value of the material.
  The commenter is also incorrect in
 asserting that the approach used in
today's rule  is inconsistent with that
used in the Petroleum Refining
 proposal. In that proposal the Agency
evaluated landfill disposal for many of
the wastes examined, because, in fact,
this practice was reported to occur for
those wastes. Contrary to what the
commenter implied, EPA did riot project
landfill disposal in the Petroleum

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64384    Federal Register/Vol. 63, No. 223/Thursday, November  19,  1998/Rules and Regulations
Refining proposal as plausible for
wastes that had no evidence of such
disposal.
  The commenter also stated that the
Agency violated its own risk assessment
criteria as presented in the listing
determination for the proposed Dyes
and Pigments wastes (see 59 FR 66076).
The commenter pointed out that EPA
states in the preamble that it is the
Agency policy that a high-end hazard
quotient above 1 represents a risk level
for presumptive listing, and a high-end
hazard quotient above 2 is a definite
basis to list. The commenter argued that,
if EPA applies this policy to the solvent
listing determination, at a minimum -
both acetonitrile and 2-methoxyethanol
have hazard quotients exceeding this
criteria (HQ of 200 and  16. respectively),
and should have been listed.
  EPA disagrees that its decisions in
today's listing are inconsistent 'with its
listing policy. As the Agency explained
in the proposed rule, EPA's risk
assessment for acetonitrile indicated
HQs below one at the bounding level for
incineration and at the high-end for
wastewater treatment tanks and for open
storage tanks. EPA's risk assessment for
2-methoxyethanol indicated HQs below
one in bounding analyses for
wastewater treatment tanks and
incineration and no risk for the storage
tank scenario. The HQs cited by the
commenter were reported as part of an
intermediate stage of the analysis, as
reported in the background document
for the proposed rule, specifically, §5.7
of the Assessment of Risks from the
Management of Used Solvents. This
intermediate stage was used to decide if
further evaluation was necessary.
Because possible risks of concern were
found, EPA proceeded to a third phase
of assessment. After consideration of the
fact that nearly all of the wastes
evaluated in the intermediate analyses
were already hazardous, EPA's
assessments for these scenarios
indicated risks below levels of concern
for the remaining nonhazardous waste
streams (see Supplemental Risk
Assessment). These multi-phase
assessments are discussed further in
response to specific comments on
acetonitrile in section IV.D.3 of today's
document.
4. Plausible Mismanagement Scenarios
  Two commenters stated  that EPA
relied on incomplete data provided in
the RCRA 3007  Questionnaires to
identify actual management, and
disregarded standard potential
mismanagement scenarios based on an
incorrect assumption that solvent waste
management will  not change over time.
According to these two commenters, a
valid solvent listing determination must
also consider improper disposal in
unlined landfills, impoundments, waste
piles, land treatment units, and long
term accumulation, which EPA
overlooked. One of the commenters
went on to state that the Agency's listing
policy requires the presumption of land
disposal in unlined landfills and surface
impoundments, particularly in the case
of solvents, where EPA's questionnaire
data present a partial and misleading
snapshot of solvent use due to
limitations in the data collection
methodology. This commenter also
argued that due to the  limitations of the
data collection, EPA cannot claim that
the specialized or limited uses of the
solvents lead to a complete
characterization of solvent users or
solvent waste management practices.
The commenter concluded that EPA's
decision not to list these solvents is
invalid and contrary to the criteria
enumerated in 40 CFR 261.11.
  The Agency disagrees with the two
commenters. The data collected show
that the management practices of most
concern to the commenters  (landfills
and surface impoundments) are not
widely used. Where land-based disposal
was reported in the 3007 Survey, the
Agency considered whether the waste is
capable of posing a substantial'present
or potential hazard to human health or
the environment. For landfills, EPA
found that modeling was not necessary
because solvent loadings were very low.
The few cases of surface impoundment
use were fully evaluated via modeling
and were found to present no significant
risk.
  EPA relied on management practices
reported in response to the 3007
Surveys, and EPA evaluated the
potential risks associated with those
management practices that are used or
likely to be used. As the Agency has
explained in prior responses, EPA could
and did target the facilities and
industries actually using these
chemicals as solvents. As a result, the
Agency identified the largest users of
these chemicals as solvents. EPA has
responded in detail to comments
regarding the adequacy of the
characterization of solvent waste
generators earlier in today's document
(see section IV.A.I).
  The solvent wastes reported from the
Survey fell into several classes: high
concentration organic  liquids or solids,
treatment residuals (wastewater
treatment sludge, incinerator ash),  and
wastewaters. The high content organic
nonwastewaters were sent to thermal
treatment in incinerators, boilers, or fuel
blenders, and in some cases recovered
via distillation for reuse. The vast
majority of these wastes were managed
as hazardous waste, because they
exhibit a characteristic (primarily
ignitability), or they are generated as a
waste mixture with solvents that are
already listed as hazardous. "
  From the data available, EPA
evaluated the potential for risks to arise
from disposal of solids in landfills and
the treatment of wastewaters in surface
impoundment. Wastes reported to go to
landfills were typically treatment
residuals that contained negligible
amounts of solvents. For the 10 solvents
examined (the remaining 4 on the
original list of 14 had essentially no
solvent use), no landfill disposal was
reported for six of these solvents. In fact,
of the total 435 solvent wastes reported
for the 10 chemicals, only 5 were
reported to go to  nonhazardous waste
landfills. In the proposed rule and the
Listing Background Document, EPA
discussed why the few cases of landfill
disposal reported for specific solvents
(acetonitrile waste, methyl  chloride,
cumene, and cyclohexanol) were not of
concern. This was principally because
the solvent loadings in these wastes
were very low. In response to
comments, EPA further considered one
waste that was reported to be disposed
in a hazardous landfill. However as
discussed in the specific section in
today's rule on acetonitrile, the waste is
no longer going to any type of landfill
due to its thermal value.
  The Survey data show that wastes
sent to landfills contained negligible
amounts of solvent; landfilling of wastes
with high solvent concentration was not
reported. Thus, given these results, and
the fact that nonwastewaters with high
solvent content are generally hazardous
and could not be placed in even a
Subtitle C landfill without further
treatment, EPA had no reasonable basis
to conclude that disposal of spent
solvent wastes in landfills poses a risk
of concern.
  Similarly, treatment of wastewaters in
surface impoundments was rare for the
solvent wastes examined (the vast
majority were treated in tanks). Of all
the wastes reported (435), only 10 were
reported to undergo treatment in surface
impoundments. The solvent loadings for
six of these (from solvent use of
acetonitrile and cumene) were low and
clearly present no risk after dilution/
treatment in a wastewater treatment
system. The others were larger volume
wastewaters that arose from the
specialized use of three different
solvents: methyl  chloride, phenol, and
furfural. With the reported solvent
loadings available, EPA examined these
special cases closely, and completed
further modeling in response to

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           Federal Register/Vol. 63, No.  223/Thursday,  November  19,  1998/Rules and Regulations    64385
comments (see section IV.C. 1 on surface
impoundment modeling).
  Concerning storage in waste piles and
land treatment, EPA found no cases
where such management practices were
reported for any of the wastes examined.
The lack of waste pile storage is not
surprising given the nature of most
wastes that are accumulated, i.e.,
organic liquids and aqueous
wastewaters, which are stored in tanks.
Further, many of these wastes are
already hazardous, and are therefore
kept in storage containers that meet
stringent RCRA regulations. Other solids
were either relatively low volume
wastes, for which a pile is not needed,
or wastewater treatment residuals,
which have no appreciable solvent
content, as noted above. The practice of
land treatment is a special practice that
is relatively rare, and as EPA has noted
in the past (see Dyes and Pigments rule,
59 FR 66074), such practices would be
considered plausible only when
information indicates that the practice is
in use, or likely to be used in the future.
  The Agency determined that the
actual management practices represent
the plausible management practices for
the specific solvent wastes that are the
subject of  today's rule, because the
Agency found no reason to believe that
the current management practices
would change significantly. In the case
of wastewaters, EPA has no reason to
believe that a facility would convert
from a tank-based system to a surface
impoundment given the capital
investment and liability issues
associated with constructing and
operating land-based treatment units.
The ongoing operating costs of
managing  wastewaters in an already
installed tank are quite small relative to
the costs of constructing a surface
impoundment, or the costs of other
alternatives such as sending the
wastewaters offsite. Clearly, a large
majority of facilities perceive a benefit  .
from managing the waters in tanks,
rather than impoundments, and EPA
finds no reasons to project that those
facilities would change their practices.
For nonwastewaters, EPA has no reason
to believe  that a facility would switch
from the thermal treatment of high
organic wastes to disposal in a
nonhazardous landfill  due to the BTU
value and  the liability issues associated
with land-based disposal. In fact, the
data collected from the Survey clearly
show that  the use of impoundments and
landfills is rare, and such practices are
not common for these wastes. Also, as
noted previously, the vast majority of
nonwastewaters are already classified as
hazardous waste, and cannot be land
 disposed without meeting treatment
 standards.
   EPA believes the Survey did, in fact,
 collect sufficient data from the
 significant solvent users, to allow a
 reasonable assessment of plausible
 mismanagement scenarios. However,
 even assuming the data do not reflect all
 management practices for whatever
 reason, the Agency still maintains that
 the data available support  EPA's
 decisions on what constitutes plausible
 mismanagement. The data collected
 show that the management practices of
 most concern to the commenters
 (landfills and surface impoundments)
 are rarely used for these solvent wastes.
 Furthermore, when these practices are
 used they are used for only very dilute
 concentration (and low risk) solvent
 wastes, except for a few special cases
 that were specifically considered by the
 Agency. The existing data  do not
 support the commenters' argument that
 other practices must  be assumed to be
 generally plausible for all the wastes
 evaluated. Creating hypothetical waste
 management scenarios would have no
 apparent benefit, and may  lead to
 regulating wastes which do not present
 risks.
 C. Risk Assessment
  This section deals with comments on
 the hazard and exposure assessments
 conducted for the rulemaking. In
 response to comments, the Agency
 revised the risk assessment for some
 management scenarios. These updated
 results are presented in the following
 sections, along with responses to the
 comments. Full details of the updated
 analyses are presented in the
 background document for the risk
 assessment (Assessment of Risks from
 the Management of Used Solvents:
 Supplemental Risk Assessment
 Background Document, hereafter known
 as Supplemental Risk Assessment)
 provided in the docket to this rule. A
 summary of risk assessment results for
 all solvents are shown in Table 3.
 Comments dealing with the volumes
 and concentrations of wastes used as
 inputs for the risk assessment are  dealt
 with in sections IV.A and IV.B.

 1. Surface Impoundments
  EPA received a variety of comments
 relating to the assessment of risks from
 management of solvent wastewaters in
surface impoundments. One comment
focused on the routes of exposure that
were assessed from the groundwater
 pathway from surface impoundments.
The commenter indicated that EPA's
consideration of direct ingestion alone
was insufficient for assessing the risk
from this pathway, and suggested that
 the Agency evaluate other routes of
 exposure from groundwater. EPA agrees
 that these additional routes of exposure
 should be evaluated, and conducted
 additional analysis as described below.
   In addition, two commenters
 suggested that the risk assessment
 should have assumed  a higher
 concentration level for the solvents in
 these management units. The Agency
 used the headworks concentration (at
 the beginning of the wastewater
 treatment process), which represents a
 dilution of the solvent with other
 wastewaters. The high-end data on
 concentrations were taken from the
 section 3007 survey of all facilities, as
 noted in section IV.B.2, above.
   EPA does not agree that higher
 concentrations of solvents should be
 used, but rather believes that its
 approach described below is more
 appropriate. To respond to these
 comments, the Agency conducted
 further modeling of surface
 impoundments to reevaluate the risks
 from solvents managed in these units.
 The risk reevaluation is summarized
 below; see the Supplemental Risk
 Assessment document for a full
 description of the methodology and
 results.
   In the risk assessment for the
 proposed rule, EPA reviewed the high-
 end waste streams going to surface
 impoundments. The process of iterative
 risk screening rests on assessing high-
 end values, based on the premise that
 low-end values represent lower risk.
 Since the high-end waste streams did
 not show significant risk, EPA did not
 review the impoundments further. For
 the current effort, EPA ensured that all
 relevant factors were accounted for by
 modeling all the surface impoundments
 receiving wastewaters  with these
 solvents. EPA used a standard Agency
 model (CHEMDATS) to assess the
 steady state concentration of solvent in
 these units; EPA used the precursor
 (CHEMDAT7) in modeling for the
 proposed rule. To the extent possible,
 EPA attempted to use actual influent
 concentrations into the impoundments;
 this information was only available for
 one of the impoundments (at the Exxon
Baytown facility). For the other surface
 impoundments, EPA used the
headworks concentrations again. EPA
believes that these concentrations
represent a conservative estimate of the
concentration of solvent entering the
impoundment, since they do not
account for the significant pretreatment
occurring (in all cases) after the
headworks, before entering the
impoundment. Because of this
pretreatment, the actual solvent
concentration of influent to the

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64386    Federal Register/Vol. 63, No.  223/Thursday,  November 19,  1998/Rules and Regulations
impoundment will be much lower than
the headworks concentrations that were
assumed for the modeling.
  Using CHEMDAT8, EPA then
modeled the resulting steady state
concentrations of the solvents in each
impoundment, as well as estimated
quantities and concentrations of
solvents that would be emitted to the
air, EPA assessed direct inhalation risks
using these airborne emissions from the
solvent.
  Risks from the groundwater pathway
were assessed for all impoundments
where the groundwater was considered
at risk. To assess the risks from the
groundwater pathway, EPA assumed no
attenuation from the impoundment to
the leachate. EPA estimated
groundwater concentrations at a high-
end receptor, and from that groundwater
pathway assessed risks of direct
ingestion of the groundwater, as well as
inhalation and dermal contact risks
from use of the groundwater. This
assessment used the same methodology
employed by the Agency in a recent
listing (Hazardous Waste Management
System; Identification and Listing of
Hazardous Waste; Petroleum Refining
Process Wastes; 63 FR 42109, August 6,
1998 ) to estimate non-ingestion risks
from the groundwater pathway.
  The results of the assessment for the
impoundments  are summarized in Table
2. All hazard quotients represent
cumulative figures for all pathways and
routes of exposure. The assessment of
cumulative risk from these routes of
exposure is very conservative, in that it
assumes that receptor locations were at
the maximum exposure point for direct
inhalation of airborne solvents, as well
as for exposure to solvents in
groundwater. EPA also added HQs from
different chemicals in the same unit,
making the highly conservative
assumption that all of the
noncarcinogens threatened similar
health endpoints (i.e., cause the same
type of damage to the same organs). This
latter assumption is not likely to be true,
but there was no need to refine the risk
analysis to ascertain what the different
endpoints might actually be, because
the summed HQs were less than one.
Because those multiple conservative
assumptions were used in the analysis,
the true high-end risk estimates would
actually be  lower than the numbers
listed under the "High-End" column.
        TABLE 2.—RISK ASSESSMENT RESULTS FOR MANAGEMENT OF SOLVENTS IN SURFACE IMPOUNDMENTS 1
Facility
Tennessee Eastman 	
Exxon Baytown . 	
Mobil Beaumont 	
Lyondcll . . . . . . ..
Rhone-Poulenc . . 	
Citao 	
Solvents in unit
Acetonitrile, Phenol 	 	
Methyl Chloride2 .
Furfural, Phenol 	
Cumene 	 . ...
Acetonitrile 	
Phenol, Furfural 	
Bounding HQ2
3.30&-02
[4 60e-06]
1.20e-fOO 	
4 ioe-02
652e-02
7.40e-01 	
"High-end"
HQ2
N/A3.
[3 50e-06]
8.00e-01 .
N/A
N/A
N/A.
  1 Risks presented represent the total risk from concurrent exposure to air and groundwater releases, and also the sum of risks from all solvents
in the unit. The "high-end" risks are above a high-end due to these and other conservative assumptions.
  2 Risks for methyl chloride represent excess lifetime individual cancer risk .
  3 N/A indicates high-end analysis was not done because the bounding analysis showed no risk of concern.
2. Tank-Based Management of Wastes
  In the process of responding to
comments comparing EPA's evaluation
of the solvent wastes in question with
the results of a recent EPA study on
potential air risks (see comment below
related to the Air Characteristic Study),
EPA reviewed the risk analyses
conducted in the proposed rule for
management of wastes in tanks.  EPA
discovered that an arithmetic error was
made in the  calculation of solvent
emissions from tanks. This error
resulted in an underestimation of
emissions for all tank scenarios by a
factor of 1,000.
  EPA has therefore revised the risk
estimates for tank-based management of
wastes. The analytical approach was to
update the analyses that were
completed for the proposed rule, using
corrected emissions, the latest version of
the emissions model (CHEMDAT8), and
current chemical and toxicological
benchmark data available for some
chemicals. The analysis also refined
parameter values to more closely
approach high-end analyses;
nevertheless, because of multiple high-
end assumptions, all of the revised
analyses are still characterized as more
conservative than true high-ends. In
addition, EPA conducted a second
analysis to verify these results. This
second analysis used air dispersion data
and receptor distances from EPA's Air
Characteristic Study (May, 1998). Both
analyses, using the corrected source
term data, indicated that risks for all
tank-based scenarios were below levels
of significant concern (see section IV.C
for further discussion of listing
decisions). More details of the analyses
are presented in the Supplemental Risk
Assessment Background document. The
results of these analyses are presented
in Table 3.
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Federal Register/Vol. 63, No. 223/Thursday,  November 19, 1998/Rules and Regulations    64387
Table 3. Summary of Risk Assessment Results for All Solvents Examined
Solvent
Furfural
2-Methoxy-ethanol
acetate
Cumene
Cyclohexanol
2-Ethoxy-ethanol
acetate


Isophorone

Management
Scenario
Surface
impoundment
Aerated WWT
tank
On-site accumul.
Incineration
On-site accumul.
Incineration
Surface
impoundment
Aerated WWT
tank
On-site accumul.
Incineration
On-site accumul.
Incineration
Aerated WWT
tank
On-site accumul.
Incineration
On-site accumul.
Incineration
Exposure
Route
Inhalation
Groundwater
ingestion
Groundwater
non-
ingestion
Inhalation
Inhalation
Inhalation
Inhalation
Inhalation
Inhalation
Groundwater
ingestion
Groundwater
non-
ingestion
Inhalation
Inhalation
Inhalation
Inhalation
Inhalation
Inhalation
Inhalation
Inhalation
Inhalation
Inhalation
HQ'2
Bounding
5.7E-01
3.3E-01
1.3E-01
-
—
1.2E-14
—
7.3E-13
3.1E-03
1.3E-06
1.4E-04
-
—
6.4E-09
—
1.3E-08
—
—
2.2E-08
—
2.3E-08
High-End
1.1E-01
3.3E-01
1.3E-01
9.0E-01
I.OE-05
—
9.0E-05
—
~
— .
—
2.4E-04
l.OE-02
~
8.0E-01

1.4E-04
2.0E-01
—
l.OE-02
—
Verification
Analysis
(Air Characteristic
Study methodology)
—
-
—
6.0E-01
5.0E-07
—
9.0E-05
..
—
—
—
1.9E-04
6.0E-03
—
9.0E-01
—
6.1E-05
5.0E-01
—
2.0E-01
— •

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64388    Federal Register/Vol. 63, No. 223/Thursday, November 19,  1998/Rules and Regulations
Methyl chloride2
2-Methoxyethanol
Phenol
Acetonitrile
Surface
impoundment
Aerated WWT
tank
On-site accumul.
Incineration
Aerated WWT
tank
On-site accumul.
Incineration
Surface
impoundment
Aerated WWT
tank
On-site accumul.
Incineration
Surface
impoundment
Aerated WWT
tank
On-site accumul.
Incineration
Inhalation
Inhalation
Inhalation
Inhalation
Inhalation
Inhalation
Inhalation
Inhalation
Groundwater
ingestion
Groundwater
non-
ingestion
Inhalation
Inhalation
Inhalation
Inhalation
Groundwater
ingestion
Groundwater
non-
ingestion
Inhalation
Inhalation
Inhalation
4.6E-062
-
—
[3.3E-14]
-
N/A3
3.6E-08
1.7E-01
1.4E-03
2.4E-02
-
--
7.4E-03
1.1E-02
1.1E-02
7.0E-02
-
- .
6.1E-07
3.5E-062
[1.3E-06]
[4.0E-06]
—
3.0E-02
—
—
-
--
—
4.6E-03
4.0E-01
—
—
—
—
1.8E+0
4.0E-01
—
3.5E-062
[4.8E-07]
[2.0E-06]
-
1.3E-02
-
-
—
—
—
1.9E-03
4.0E-02
~
—
-
—
7.3E-01
7.0E-01
-
       1 The "high-end" risks are above true high-end values, because multiple high-end assumptions make the analyses
       more conservative than true high-ends.  z Risk numbers for Methyl Chloride represent excess lifetime individual
       cancer risk 3 All wastestreams being accumulated are already regulated as hazardous wastes.
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            Federal Register/Vol. 63. No.  223/Thursday, November  19,  1998/Rules and Regulations    64389
 3. Multiple Solvents
   A commenter noted that EPA failed to
 consider the cumulative impacts of
 multiple solvents and other hazardous
 constituents released via the same
 exposure pathways in the risk
 assessment. In order to fully respond to
 this comment, EPA conducted an
 assessment of the cumulative risks
 posed by exposure to multiple solvents.
 Inasmuch as the listing determination is
 based on the solvent constituents of
 these wastes, other constituents of the
 wastestreams were not assessed. These
 risk assessment results, therefore, only
 apply to the solvents themselves.  In this
 analysis (see the Supplemental Risk
 Assessment for details) EPA assessed all
 cumulative solvents risks where
 multiple solvents were managed in one
 unit or in different units at a facility.
   This analysis used the same
 assumptions as EPA's prior assessments
 for the proposed rule. Wastestreams
 which were already classified and
 managed as hazardous were not
 assessed, since there is little likelihood
 of risk reduction through a listing
 determination. EPA focused its effort on
 currently unregulated wastes. The
 characterizations of waste  management
 included the same conservative
 parameters as in the proposed rule,
 modified as described above, including
 the construction and operation of
 surface impoundments, meteorological
 conditions, and the proximity of
 hypothetical receptors. One particularly
 conservative assumption was storage of
 solvents in open-topped tanks
 permitting maximum volatilization.
 This assumption of extensive
 volatilization out of open-topped tanks
 is highly unlikely, because the wastes
 were being stored pending incineration
 or other thermal treatment. In addition
 to those factors, EPA included highly
 unrealistic assumptions in assessing
 cumulative risk from exposure to
 multiple solvents. Environmental
 receptors were considered  to be located
 at maximum exposure points relative to
 all management units. EPA also added
 HQs from different chemicals, making
 the highly conservative assumption that
 all of the non-carcinogens threatened
 similar health endpoints (i.e., cause the
 same type of damage to the same
 organs). This latter assumption is not
 likely to be true, and overestimates
 risks, but there was no need to refine the
 risk analysis to ascertain what the
 different endpoints might actually be.
  Despite these assumptions, which
suggested unrealistic conditions to
maximize the probability of showing
risk to human health, none of the
assessed scenarios showed combined
 hazard indices over one. In one facility
 (Exxon, Baytown), a surface
 impoundment showed an increased
 cancer risk of 4E-06 in the high-end
 analysis, however, this risk was entirely
 due to the single solvent methyl
 chloride, as shown in the preceding
 section. As discussed in section IV.D,
 EPA has concluded that this does not
 represent a significant risk, especially in
 light of existing air regulations that
 apply to this unit.
   The scientific evidence represented
 by this risk analysis leads EPA to the
 clear conclusion that management of
 multiple solvents does not pose
 significant incremental risk to human
 health in any populations.
 •4. Comparison With HWIR Exit Levels
   A commenter argued that EPA should
 reconsider the risks from acetonitrile,
 phenol,  methyl chloride, and
 isophorone based on the risk analysis
 presented by EPA in the proposed
 Hazardous Waste Identification Rule
 (HWIR; 60 FR 66344. December 21,
 1995). For each of these chemicals, the
 HWIR analysis produced an "exit level"
 concentration, suggesting that
 concentrations of waste higher than the
 exit level might pose unacceptable risks.
 The commenter notes that the §3007
 survey showed solvent wastes for each
 of these chemicals being generated at
 higher concentrations than the HWIR
 exit levels. The commenter noted that
 wastewaters of acetonitrile, phenol,
 methyl chloride, and isophorone are
 generated in concentrations higher than
 the HWIR exit levels for these'
 chemicals.
  The commenter's comparison
 between HWIR exit levels and the
 solvent waste concentrations does not
 indicate  that the solvent risks are of
 concern. The purpose of the HWIR exit
 levels is  not to assess risk from a
 particular set of chemicals or a specific
 set of wastes. Unlike listings, where the
 Agency makes a decision  based on
 actual information about how specific
 wastes are generated and managed, the
 HWIR levels are intended as broad risk
 screens, covering a large number of
 possible waste streams and waste
 management methods. The listing
 decisions for the chemicals examined in
 today's rule are limited to consideration
 of potential risks that arise 'only from
 the wastes generated after the chemicals
 are used  as solvents. Therefore, these
decisions are limited to considerations
 of waste characteristics and waste
management practices specific to these
uses.
  Because HWIR had a different
purpose than this risk assessment, it
used different methodologies. HWIR
 evaluated five management scenarios:
 aerated treatment tanks, quiescent
 surface impoundments, land application
 units, ash monofills, and wastepiles.
 Only two of these scenarios aerated
 treatment tanks and quiescent surface
 impoundments are similar to the
 management scenarios modeled for the
 used solvents risk assessment. Another
 obstacle to comparison is the waste
 volume modeled. HWIR modeled a
 range of waste volumes, bounded by the
 capacity of the waste management unit.
 From these volumes, HWIR calculated
 levels for specific chemicals on a
 nationwide basis, for any use in any
 industry, and made various assumptions
 for waste generations and management,
 as noted above. In contrast, the
 wastestream volumes (and constituent
 loadings) modeled for the solvents risk
 assessment were based on actual data
 from the industry survey.
   The Agency has not issued the HWIR
 in final form and is continuing to refine
 the analysis; therefore, the HWIR exit
 levels are currently being reviewed and
 revised. However, even the revised
 numbers, as a screening tool, cannot be
 automatically used  in assessing the
 validity of other regulatory actions by
 EPA. Together, the differences  in
 management units and wastes modeled
 mean that, a simple  comparison of HWIR
 exit level concentrations to the
 concentrations in modeled solvent
 wastes is not meaningful.
 5. Environmental Damage Incidents
   Several commenters stated that the
 Agency screened out and ignored
 damage cases prior to 1980. EPA
 believes that the commenters have
 apparently misunderstood how the
 Agency evaluated the damage cases. The
 Agency did not screen out and  ignore
 damage cases prior to 1980. All damage
 cases available were considered
 including those prior to 1980, However,
 most of the damage  cases found for the
 14 chemicals resulted from disposal
 well before 1980, before RCRA
 regulations were in place. Damage cases
 were reviewed to direct the analysis to
 industries and conditions that might
 show evidence of environmental
 damage from improper management of
 used solvents that might be occurring
 now or may occur in the future; the
 cases did not provide an exclusive or
 restrictive guide. EPA evaluated a
 variety of legal and financial factors that
 might affect plausible management, and
 technological factors affecting fate and
 transport of hazardous constituents.
  These other factors are especially
 important when examining the solvent
wastestreams, since almost 90% of the
non-wastewaters are already required to

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64390    Federal Register/Vol.  63,  No. 223/Thursday, November 19, 1998/Rules and Regulations
be managed as hazardous under Subtitle
C. Although these constituents may
have been found at Superfund sites, it
Is not reasonable to suggest that RCRA-
regulated hazardous wastes could be
managed today in the same way they
were managed at industrial facilities in
the past. The damage cases that were
found reflect mismanagement in the
past, not the Subtitle C management (or
even the likely Subtitle D management)
of these chemicals which is the norm
today.
  Furthermore, as described in  the
proposed rule, there were many other
reasons why the damage cases were not
useful (see 61 FR 42326). These reasons
include: (1) EPA could not determine
that any of the contaminants of concern
were" used as a solvent prior to disposal;
(2) wastes at these sites were poorly
defined, and the term "solvent wastes"
likely referred to the more widely used
solvents that are already listed;  (3) many
of the chemicals under study have other
uses that are more likely to be the
reason for contamination; and (4) EPA
found no damage cases at sites within
the industries that reported using the
solvents under study.
6. Spills, Leaks, and Overflows
  One commenter stated that EPA's risk
assessment did not include an
evaluation of human health and
environmental risks posed by leaking
tank systems. According to this
commenter. EPA argues the
concentration of solvents is "very low"
in wastewaters, and thus assessing the
risks posed by tank leaks is not
warranted. However, the commenter
argued the database identifies solvent
wastewaters containing 9% 2-
methoxyethanol. 8% phenol, 200 ppm
2-EEA, 169 ppm methyl chloride, and
5,000 ppm furfural. The  commenter
concluded, given that no time limit
would be placed on storage if the wastes
are not regulated as hazardous,  defective
leaking containers and tanks are highly
possible.
  EPA has examined the possibility of
spills from management units such as
tanks or surface impoundments. The
Agency does not have the data  or the
means available to accurately assess the
likelihood of such releases, the
magnitude of releases, or other  data that
would be necessary to assess the risk of
such spills. Based on the characteristics
of these solvent waste streams,  however,
the Agency has concluded that to the
extent that such releases would pose
risks, a decision to list any of these
wastes would not provide significant
reduction in the potential hazards from
such events. The Agency bases that
conclusion on the following facts.
  The vast majority (over 98%) of the
volume of solvent wastes are
wastewaters in wastewater treatment
units. These wastewaters are diluted to
very low concentrations of solvents, and
are treated further to even lower levels.
When necessary, EPA has modeled the
effects of release of some of these
solvents from impoundments and found
no significant risk to human health or
the environment (see section IV.C. 1  for
further discussion on potential risks
from impoundments). For the specific
wastewaters identified by the
commenter, EPA notes that surface
impoundment scenarios were modeled
for phenol, methyl chloride, and
furfural at the same or similar
concentrations to those cited, and no
significant risks were found. The
wastewater mentioned that contains 2-
methoxyethanol is managed as
hazardous in an off-site biological
treatment system, so that any releases or
risks are unlikely. Similarly, the 2-EEA
waste cited is scrubber water that is
classified as hazardous, and furthermore
corresponds to a total of only 0.58 kg of
EEA. Therefore, EPA does not  agree that
these wastes are likely to present
significant risk even under a spill
scenario.
  Of the nonwastewaters, almost 90%
are already regulated under Subtitle C of
RCRA. Spills from the RCRA units are
already covered under contingency
planning and corrective action
requirements. Subpart CC includes
additional requirements for spill
protection during transfer of wastes (see
40 CFR 264.1084Q)). Therefore, EPA
concludes that spills of these wastes
from tanks, which would generally be
episodic in any case and unlikely to
produce long-term exposures
comparable to those considered in
listing determinations, are not of
significant concern.
7. Non-Aqueous Phase Liquids (NAPLs)

  In the proposed rule, even though
EPA could not find scenarios that could
lead to significant releases to ground
water, the Agency also considered
whether the spent solvent wastes had
the potential to form non-aqueous phase
liquids (NAPLs) that might move as a
separate phase either above or below the
ground water table. These NAPLs may
present special problems, especially in
assessing their transport  and potential
impact. However, EPA found that nearly
all solvents under consideration are
miscible or very soluble  in water and
are not likely to form NAPLs in
groundwater. One commenter suggested
that  EPA re-examine the possibility of
formation of NAPLs from these solvents.
  To respond to this concern, EPA has
conducted further analysis on the
subject for this final rulemaking. Full
details of this analysis are in the
Supplemental Risk Assessment
document for this rulemaking. Only four
of the solvents are land disposed and
pose a threat to the groundwater
pathway: acetonitrile, phenol, furfural,
and cumene. EPA assessed the
possibility of formation of NAPLs from
land disposal of these solvents.
  The first three are all highly soluble,
which indicates that NAPL formation is
unlikely. EPA then assessed the
likelihood of NAPL formation from
cumene, using the methodology which
has been developed for assessing NAPL
probabilities at Superfund sites.
Conservative estimations of the
concentrations of cumene in
groundwater still fell an order of
magnitude below the threshold at which
NAPL formation is a serious possibility.
Therefore, EPA concludes that there is
little likelihood of these solvents
contributing to formation of NAPLs.
8. Risk Modeling Parameters
  One commenter stated that the
accumulation scenario modeled must
assume long term storage, not a period
of under 90 days. The commenter
argued that extended on-site
accumulation is a highly plausible
mismanagement scenario, given that
absent RCRA controls, a generator can
accumulate such waste indefinitely.
Thus, the commenter stated that EPA's
risk model should not assume a finite
storage time of 90 days, but should
assume the more likely scenario of at
least a two year period of storage.
  This comment is based on an
incorrect assumption. The accumulation
scenario was not modeled for a period
of 90 days as stated by the commenter.
For each scenario, EPA used a storage
duration designed to maximize the total
risk. Modeling a longer storage time
does not necessarily increase the risk,
because it implies less frequent refilling
of the tanks with new wastes. As
described in the risk assessment
documentation, this storage duration
time was calculated by first generating
a tank profile to yield the largest
downwind concentration at the nearest
residence based on data in Hazardous
Waste Treatment, Storage, and Disposal
Facilities (TSDF)— Background
Information for Proposed RCRA Air
Emission Standards (referenced in the
proposal risk documentation as U.S.
EPA, 1991c; p. 29, July 1996). (This
high-end tank  also happened to be the
most common. Therefore, this model
tank was used for all three types of
estimates: bounding, high-end, and

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             Federal  Register/Vol. 63, No. 223/Thursday. November 19, 1998/Rules and Regulations     64391
  central tendency.) The throughput and
•  other parameters of this model tank
  were used in combination with solvent
  throughputs and high-end and central
  tendency concentrations to obtain
  solvent-specific emissions rates. The
  storage duration times were then back-
  calculated to fit this maximum release
  profile. For the bounding analysis, the
  modeling was so conservative that it
  resulted in greater than 95 percent
  release of the solvent in seven out of ten
  cases. Thus, a longer accumulation time,
  as suggested by the commenter, would
  have led to lower emissions, lower
  concentrations at the receptor, and thus
  a less conservative analysis.

  9. Comparison With Results of Air
  Characteristic Study
    EPA received a late comment
  suggesting that the risk analysis in the
  Air Characteristic Study recently
  released by the Agency (May, 1998)
  indicated that air pathway releases from
  these solvents were riskier than EPA's
  initial analysis had  indicated. The
  commenter compared concentration
  levels of potential concern developed
  for some chemicals  in the Air
  Characteristic Study to concentrations
  of the solvents reported in the listing
  determination. The  commenter argued
  that the study showed significant
  inhalation risks for some of the solvents
  when managed in tanks at
  concentrations significantly lower than
  those found in the solvents data
  collection.
   In response, EPA first notes that the
  purpose of the Air Characteristic  Study
  was to evaluate the possible need for an
  air characteristic to address potential
 risks due to emissions from certain
 waste management units. The
 concentrations of concern estimated in
 the Study are screening values for the
 purpose of determining whether new
 regulatory controls are needed to  fill
 potential gaps in existing regulations,
 and should be viewed in this context.
 The concentrations developed in  the
 Study cannot be automatically used in
 assessing the validity of other regulatory
 actions by EPA, because the study uses
 waste data and certain modeling
 assumptions in its methodology that are
 different in a number of ways from the
 modeling assumptions and data used in
 other regulatory programs, such as
 listing determinations. In addition, the
 Study methodology is currently
 undergoing outside peer review.
 Therefore, the screening concentrations
 themselves could change pending the
 results of the review.
  In any event, a comparison of the
 results reached in the Air Characteristic
 Study with the results of this risk
  assessment confirms that the
  concentrations present in these solvent
  wastes do not pose a significant
  inhalation risk. As noted above, EPA
  found an error in the risk analyses for
  tanks, and revised these analyses
  accordingly. This was the principal
  reason for the apparent difference in
  risk estimates between the risk
  assessment for the proposed analysis
  and the Air Characteristic Study (see
  section IV.C.2). However, even with
  these revisions, some apparent
  differences in concentration levels of
  concern would remain.
   These differences in  concentration,
  however, do not necessarily mean
  differences in risk. In this case, the
  source terms being compared are
  different. The Air Characteristic Study
  back-calculated to determine what
  loading of constituent could be safely
  managed in a given management
  scenario. For every management
  scenario, the loadings of constituent that
  the Air Characteristic Study concluded
  could be managed safely are larger than
 the loadings used in this risk
 assessment. The solvent constituent
 loading that the Air Characteristic Study
 determined could be safely managed in
 tanks ranged from twice the amount to
 millions of times the amount modeled
 for the solvents risk assessment. The
 analyses for today's listing
 determination used the solvent waste
 generation data (and subsequent
 loadings in management units) from the
 §3007 Survey. The purpose of this
 listing is to determine the risks that may
 be posed by current and plausible future
 management of these specific chemicals
 when used as solvents, therefore, the
 EPA feels that the solvents waste
 generation data submitted from the 3007
 survey is appropriate to use in the
 analysis.
,   To better understand the differences
 in risk assessment methodology used in
 the Air Characteristic Study, the Agency
 conducted a re-analysis  of the risk from
 the solvent wastestreams using a
modified methodology from the Air
Characteristic Study, but still using the
waste generation data and solvent
loadings from the listing Survey. The
methodology was virtually the same as
that used in the Air Characteristic
Study, except for some inputs that the
study derived through Monte Carlo
analysis. The results of this verification
analysis showed no significant risk for
any of the solvent management
scenarios, and confirm the previous
results. These results appear in Table 3.
More details on these comparisons
appears in the response to comments
document accompanying this
rulemaking.
  D. Listing Determinations
    EPA received comments on various
  aspects of the proposed listing
  determinations. Many comments on the
  determinations were raised repeatedly
  for various wastes, and are discussed in
  preceding sections, or in sections IV.D. 1
  and IV.D. 2 below. Comments that are
  more specific for individual solvent
  wastes are addressed in the section
  IV.D.3. For complete responses to
  comments on these and other issues, see
  the Response to Comments Document in
  the docket to today's rule.

  1. General Comments
    Six commenters support EPA's
  decision not to list as hazardous waste
  the solvents at issue. However, one
  commenter disagreed with the decision
  not to list these compounds because
  they are similar in toxicity to the other
  solvents already listed as hazardous.
  The commenter stated that the solvents
  considered in this rule may be used by
  themselves, and their wastes, therefore,
  would not be mixed with the wastes
 from the other F-listed wastes, or the
 manufacturer can modify their
 processes to avoid using other F-listed
 solvents, so that their wastes would no
 longer be hazardous. The commenter
 went on to wonder if EPA's decision not
 to list these wastes was due to its "anti-
 combustion" strategy, because the
 wastes would "then be readily excluded
 from combustion as a logical disposal
 option."
   EPA does not agree with the
 commenter's assertions regarding the
 decisions not to list. While some of the
 chemicals examined in today's rule may
 have toxicity similar to the solvents
 already listed as F-wastes, the toxicity of
 a chemical alone is not a sufficient basis
 for listing. EPA considers a variety of
 factors, including waste management
 practices and all the other factors listed
 in 40 CFR 261.11 (a) (3). After evaluation
 of all factors, EPA determined that
 listing for these solvent wastes was not
 warranted. When appropriate, EPA also
 evaluated wastes that resulted from use
 of the solvent by itself and found no
 significant risks.
  Further, EPA disagrees that in the
 absence of a listing decision a
 manufacturer would change its
 processes to segregate out the solvents
 considered in this rule. They had that
 incentive from the time the other
 solvents were listed in 1980 and 1986
 and have either been mixing the wastes
ever since or made decisions to make
new mixtures with listed solvents. If a
waste is hazardous under current
regulations, due to mixture with other
listed wastes or a characteristic, the

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64392    Federal Register/Vol. 63, No. 223/Thursday, November  19.  1998/Rules and Regulations
manufacturer already has ample
incentive to modify its process to avoid
the cost of generating more hazardous
waste. These manufacturers apparendy
weighed the risks and benefits of
mixing, or not mixing the wastes and
Still pursued their mixing practices. As
the Agency has stated in today's
document and in the Response to
Comments Document, many of these
decisions are driven by specific process
parameters, cost effectiveness, chemical
compatibility, and regulations of other
Agencies, EPA has no reason to believe
they will change these practices in the
event of a final no-listing decision,
considering that this decision does not
change the status quo. Thus, EPA does
not agree that a non-list decision would
alter this behavior. Finally. EPA points
out that many of the wastes examined
in today's rule are, in fact, treated by
combustion, typically in hazardous
waste incinerators. Therefore, the
wastes are not "readily excluded" from
combustion as result of the no-list
decisions.
2. Sufficient Regulation of Solvents
   One commenter stated that EPA
assigned appropriate weight to the fact
that many solvents already are
hazardous, a determination that is
relevant to the Agency's assessment of
plausible mismanagement scenarios, its
determination in the risk assessment
that no further risk reduction could be
achieved through listing the solvents of
concern as hazardous, and its
determinations regarding the relevance
and applicability of damage incidents
identified. This commenter further
stated that EPA gave due consideration
to the benefits accorded by other
regulatory programs. Another
commenter, however, stated that the
Agency should carefully consider the
benefits associated with listing the
solvent wastes that may exhibit a
hazardous waste characteristic or are
sometimes co-managed with presently
listed solvent wastes. This commenter
stated that there are important legal and
policy reasons for listing the solvent
wastes at issue in this rulemaking. The
commenter noted that in the case  of
characteristic solvent wastes, listing the
respective wastes obviates the need for
testing to determine whether the waste
is hazardous and could facilitate
enforcement because inspectors need
only compare the waste to the listing
description to verify the applicability of
hazardous waste requirements.
   In response, the Agency notes that it
did carefully consider the impact listing
might have for solvent wastes that are
already hazardous due to the
characteristics, or mixture with
hazardous waste. For the wastes under
consideration in this rulemaking, EPA
believes that the characteristics provide
adequate regulatory control. EPA
initially evaluated potential risks from
all wastes and found risks of possible
concern due to air releases from some
wastes (for acetonitrile and 2-
methoxyethanol; see proposed rule 61
FR 42327-42332). However, the wastes
with the apparent risks were already
regulated as hazardous. After
considering the regulatory controls
required, the residual risks were found
to be below levels of concern. Based on
assessments of risks posed by these
wastes, in conjunction with the existing
regulatory controls afforded by the
existing characteristics and listings, the
Agency determined that the solvent
wastes as they are generated and
managed do not pose a threat to human
health or the environment. Therefore,
the Agency has decided  that listing is
not warranted. While listing would
obviate the need for testing (for those
wastes not already listed or mixed with
a listed waste), this is not a compelling
reason by itself to list. A listing may
assist enforcement to some extent;
however, EPA has no indication that
there is any problem in the
implementation of the characteristic
regulations for these wastes. On the
contrary, the data collected indicate that
generators are, in fact, managing the
wastes of concern as hazardous when
they are subject to such  regulations.
  The commenter states that EPA never
addresses the actual or potential
reclamation of characteristic solvent
sludges and byproducts  (See 40  CFR
261.2, Table 1). The commenter also
argued that the regulatory status of
residuals from the recovery of spent
solvent wastes are different for listed
wastes; if listed, the residuals are
hazardous, but if not listed the residuals
would be unregulated, unless they
exhibit a hazardous characteristic.
  The Agency disagrees with  the
statement that EPA did not consider
reclamation. The Agency examined all
residuals generated, including those
generated from on-site recycling
operations. Through the Survey, the
Agency collected data on actual or
potential solvent recycling and
reclamation possibilities. Among the
residuals evaluated are heavy ends,
filtrates/decantates/distillates, organic/
aqueous treated residuals, and filter
related media; these were, in  part,
generated from the recovery of spent
solvents or the treatment on-site of
spent solvent residuals.  Some facilities
have  the means and the  financial
incentive to perform reclamation of
used  solvents (often in-process). Other
facilities are prevented from performing
any sort of reclamation due to process
purity requirements and product quality
needs (e.g., pharmaceutical drugs,
semiconductors), which  may include
regulatory requirements  (e.g., purity
requirements for drugs under the Food,
Drug and Cosmetic Act). Aside from
value to fuel blenders and incinerators,
very little market seems to exist for
many spent solvents or their sludges.
While it is true that the regulatory status
of recovery residuals is different for
listed, as opposed to characteristic
hazardous waste, EPA does not believe
that this would, by itself, provide a
strong reason for listing,  unless risks can
be demonstrated for such wastes. EPA
has no data on the characteristics of
such off-site residuals, and in fact has
no indication that many of the spent
solvents at issue are sent for off-site
reclamation, beyond thermal treatment.
Furthermore, in making  a listing
determination, EPA's primary focus is
the wastes generated on-site, and not
treatment residuals that may be
generated off-site. To fully consider
these derivative wastes would expand
the scope of a listing into a much larger
effort. EPA has chosen to examine
wastes for which it can reasonably
expect to collect sufficient data to
support a listing evaluation.
  The commenter goes on to state that
in the HWIR rulemaking, EPA has not
set exit levels for most of the solvents
covered by the instant rulemaking.
Therefore, wastes may meet the HWIR
exit levels but still contain substantial
concentrations of non-listed solvents.
The commenter stated that by listing as
hazardous the solvents in this
rulemaking, EPA would  then develop
exit levels for the solvents, thus
ensuring the concentrations of these
solvents in waste mixtures are reduced
to protective levels prior to leaving the
Subtitle C regulatory system.
  The commenter is premature in
assuming the content or effect of the
HWIR rulemaking, and an assessment of
the effect of that potential rule on
residuals addressed in today's final rule
is speculative. The Agency points out,
however, that the concentrated waste
mixtures reported for the solvents at
issue are unlikely to be realistic
candidates for exemption under HWIR.
Due to the high levels of other
constituents, these wastes most
certainly have to be treated, such that
the wastes that might ultimately exit the
RCRA system would be treatment
residuals. Concentrated organic wastes
are invariably treated through
incineration or other thermal treatment,
and such treatment would likely destroy
the solvents in question, as well as the

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            Federal Register/Vol. 63, No.  223/Thursday,  November 19,  1998/Rules and Regulations    64393
 other hazardous constituents.
 Furthermore, wastes that are
 characteristic must be treated for
 underlying constituents under the Land
 disposal restrictions (LDR) regulations.
 Thus, residuals that are exempted under
 HWIR are not likely to have solvent
 levels of any concern.
   The commenter also stated that by
 listing the wastes as hazardous, EPA can
 encourage pollution prevention
 activities associated with solvent uses
 and waste management, including but
 not limited to solvent substitution,
 process changes and less reliance on
 combustion. The commenter noted that,
 through the listing process, EPA could
 ensure that the wastes will always be
 .managed as hazardous, recognizing that
 attempts to identify solvent uses and
 users in the proposal are at best,
 substantially incomplete and subject to
 change. The commenter stated that it is
 entirely plausible that pollution
 prevention programs emphasizing
 hazardous waste generation reductions,
 the increasing cost of disposal
 associated with the upcoming
 hazardous waste combustion rules, and
 other factors will encourage hazardous
 solvent waste generators to reduce or
 eliminate the use of listed hazardous
 waste solvents. Under these
 circumstances, current codisposal
 practices are not indicative of future
 mismanagement scenarios.
   The Agency believes that the existing
 regulatory requirements for these
 wastes, many of which are hazardous
 already, provide ample incentives for
 pollution prevention, both because of
 liability concerns and disposal costs
 associated with hazardous wastes. In
 addition, as noted above, under the LDR
 regulations, characteristically hazardous
 wastes must be treated for underlying
 hazardous constituents. The Agency has
 reason to believe that industry
 voluntarily'assesses opportunities for
 pollution prevention. As stated in the
 Listing Background Document (page 17),
 all but four of these chemicals are
 reportable in TRI Form R. Part of that
 reporting package includes pollution
 prevention and waste minimization. As
 an example, use of the three glycol ether
 chemicals under consideration in this
 rulemaking (2-methoxyethanol, 2-
 methoxyethanol acetate, and 2-
 ethoxyethanol acetate) has diminished
significantly, and production of 2-
methoxyethanol acetate has been
eliminated. Further, the cost of these
chemicals is high in comparison with
other comparable chemicals. These
chemicals are used in industry only
when their application is considered so
suitable as to overcome any price
disadvantages. As a result, for the
 solvents under consideration in this
 rulemaking, both regulatory
 requirements (e.g., characteristics, TRI)
 and economic factors play a role in
 encouraging companies to undertake
 pollution prevention assessments and
 institute changes where possible. Thus,
 EPA finds no  reasonable basis to project
 changes in management practices
 reported in the 3007 Survey, as
 suggested by the commenter.
   The Agency has no reason to  suspect
 that current management practices
 would be likely to change in the future
 to a practice that would pose a
 substantial risk to human health or the
 environment (e.g., from thermal
 treatment to land disposal or from a
 tank-based system to a surface
 impoundment) due to the regulatory
 prohibitions, heating value of the waste
 and/or requirements of the facility's
 wastewater treatment systems.
   The commenter also stated that EPA's
 assumption that analogous waste
 streams generated by all industry sectors
 using any of the solvents always
 generate an ignitable hazardous waste
 (based on the fact that some of the
 wastes reported to the Agency in the
 questionnaires are ignitable hazardous
 wastes), and will continue to do so, is
 not sustainable given the limitations
 associated with the preliminary and
 final questionnaires.
   EPA disagrees. Nowhere does the.
 Agency assume that analogous
 wastestreams generated by all industry
 sectors using a particular solvent always
 generate an ignitable waste. The Agency
 has determined, based on reported
 management practices, that additional
 management practices for high solvent
 concentration/high organic containing
 wastes other than those considered in
 the risk assessment are not likely to
 exist. While some solvents may exist in
 mixtures at levels that do not exhibit the
 ignitability characteristic, EPA assessed
 risks from such mixtures as reported in
 the 3007 Survey. In fact, the initial risk
 analyses for all solvents did assess the
 risks from the wastes reported to be
 hazardous. Except for the cases of
 acetonitrile and 2-methoxyethanol, EPA
 did not pursue the impact of the
 hazardous waste designations, because
 the risk results for the other solvents
 were below levels of concern. In the
next phase of risk analyses for
 acetonitrile and 2-methoxyethanol, the
Agency did not find significant risks
from any remaining nonhazardous
wastes. (See Supplemental Risk
Assessment document for more details.)
  The Agency  found that process and
other limitations are a technical and
regulatory bar to using the 14 chemicals
alone or in combination with non-listed
 solvent wastes. For example, FDA
 regulations preclude solvent
 substitution in the pharmaceutical
 industry. Similarly,  chemical purity
 concerns and final product quality
 requirements often specify the
 chemicals to be used.
   Another commenter stated that EPA
 had wrongly assumed that the 10
 solvent wastes are already captured as
 hazardous by the characteristics. The
 commenter states that four of the ten
 solvents of concern have flash points
 that do not meet the characteristic of
 ignitability: phenol,  isophorone, furfural
 and cyclohexanol. Wastes from these
 four chemicals could never exhibit the
 characteristic of ignitability, unless
 generated in mixtures with some other
 component that has a low enough flash
 point. Two commenters provided
 calculations, using Raoult's Law and the
 lower flammability limit, of the
 potential concentration of solvents in a
 mixture that would result in an ignitable
 waste. These commenters contend that
 the solvent concentration in the
 mixtures must be very high to produce
 a mixture that is ignitable.
   As noted above,  EPA did not need to
 rely on the fact that all waste mixtures
 would be ignitable. Certainly for the
 four solvents mentioned by the
 commenter, EPA did not rely only on
 the hazardous waste  designations, but
 rather presented risk results for all
 wastes reported. In addition, the amount
 of solvent in nonwastewaters for two of
 the chemicals cited were extremely
 small (cyclohexanol-16 kg; furfural-
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64394    Federal Register/Vol. 63, No.  223/Thursday,  November 19, 1998/Rules  and Regulations
proposed rule and as modified by
subsequent analysis in response to
comments, EPA finds no significant
risks from treatment in aerated tanks or
combustion in a boiler. EPA concludes
that potential risks from air releases of
acetonitrile stored in open accumulation
tanks (i.e., on-site storage tanks) are also
not significant, because the vast
majority of the nonwastewater residuals
stored are already regulated as
hazardous waste. In the latter case
regulatory controls afforded by the
existing solvent listings and the
characteristics (primarily ignitability)
are protective of human health and the
environment.
  EPA's final determination not to list
this solvent is also  based on the analysis
in the proposed rule (see 61 FR 42328),
as modified by subsequent analysis in
response to comment, that potential
risks from land-based management of
acetonitrile wastes are not significant.
All wastewaters found in EPA's 3007
Survey were treated in tanks, except for
several wastes that were reported to
enter impoundments as part of a
wastewater treatment train in volumes
that would not present significant risk.
In response to comments, EPA
conducted further analysis of the
potential risks that might arise from
treatment of acetonitrile wastewaters in
a surface impoundment. This analysis
included consideration of any
additional risk resulting from
noningestion exposure from
groundwater (e.g., inhalation). As
described in section IV.C, these analyses
further confirmed this management
practice presents no significant risks
(see Table 3).
  The proposal also found that the few
wastes reported to  go to landfills
typically contained negligible levels of
acetonitrile solvents, and were not of
concern. In response to comments, EPA
further examined the potential for risks
that might arise if more concentrated
wastes were placed in an unlined
Subtitle D landfill, but continues to
believe such risks are not of concern
(see specific comments below).
   As described in section IV.B, EPA
updated its risk analysis for acetonitrile
for some management scenarios. While
the updated analyses confirmed the
evaluation in the proposed rule, the
updated analysis for aerated wastewater
treatment tanks showed an HQ of two,
which is slightly above the Agency's
presumptive no-list HQ level of one.
EPA does not believe this marginal risk
is significant for the following reasons.
First and foremost, as noted earlier in
section IV.B. the analysis that resulted
in the HQ of two is actually more
conservative than a true double-high
end analysis. The dispersion modeling
used in calculating the HQ of two
incorporates a high-end receptor
distance, in addition to two other high-
end parameters used (solvent loading
and tank scenario). Furthermore, the
solvent loading used for this analysis
was the maximum reported for
acetonitrile in wastewaters, rather than
the 90th percentile value that EPA
typically uses to estimate high-end risks
(see for example the risk analyses in the
recent Petroleum Listing, 63 FR at
42117). In the 3007 Survey for solvent
use, facilities reported the treatment of
26 acetonitrile wastewaters in tanks (see
the Listing Background Document, App.
I), and the maximum was above the
90th% value for the mass loadings from
this distribution. EPA used the second
highest loading, which was an order of
magnitude below the maximum, to see
the impact of using this value in the
updated analysis. When using the 2nd
highest loading, EPA calculated an HQ
of 0.02, or well below one. Thus, the HQ
of two is an overestimate and does not
reflect a significant risk. As further
confirmation, EPA also estimated risks
for acetonitrile wastes using the
methodology from the Air Characteristic
Study. This methodology allowed
receptor distance to be varied and was
thus closer to a true high-end analysis.
Using either the maximum acetonitrile
loading or the second highest loading,
the estimated HQ's were below 1.0 (0.7
and 0.08 respectively). Finally, EPA has
recently promulgated regulations under
the Clean Air Act (CAA) to control air
releases from the industry represented
by the one facility with the maximum
loading (September 11, 1998, 63 FR
50280). These standards control releases
of hazardous air pollutants, such as
acetonitrile, from wastewater treatment
systems at pharmaceutical producers.
Therefore, for these reasons the Agency
does not believe that the risks from
acetonitrile in wastewater treatment
tanks are likely to be significant.
  Given that nearly all of the
nonwastewater acetonitrile residuals are
either already being handled as
hazardous, and those that are not
handled that way contain negligible
amounts of the solvent, these spent
solvent residuals are not likely to pose
a significant hazard to human health or
the environment. Furthermore,
treatment of wastewaters in tanks, or in
rare cases in impoundments, presents
no significant risks. Therefore, the
Agency continues to believe that a no-
list decision is warranted.
  Specific comments. Several
commenters support EPA's no  list
decision on Acetonitrile. The
commenters confirmed that the
management practices and
characterization of wastewater and
nonwastewater residuals from the use of
acetonitrile as a solvent have been
properly identified. One commenter
also noted that the risk assessment
conducted by the Agency supports the
determination not to list acetonitrile
spent solvents. However, another
commenter disagreed with the Agency's
findings, stating that, despite
shortcomings in EPA's risk assessment,
the high-end analysis for tank storage
resulted in an estimated HQ of 200,
orders of magnitude higher than the HQ
of 1 typically warranting a hazardous
waste listing. This commenter noted
that only by performing the Phase III
assessment was the Agency able to
rationalize a no-list decision.
  In response, EPA wishes to clarify the
meaning of the different phases of the
risk assessment. The iterative process of
risk assessment began with bounding
analyses as the first phase. This type of
analysis (by definition) involves
conditions so unlikely as to be virtually
impossible. Many scenarios did not
show significant risk. Those scenarios
which showed significant risk under
bounding conditions were assessed
under "high-end" conditions in Phase
II. This was a more realistic assessment,
but still reflected close to a "worst-case"
set of conditions.
  Of all scenarios evaluated for
acetonitrile, only one showed
significant risk when modeled under
high-end conditions, an uncovered
storage tank (also called on-site
accumulation in the proposal). The
commenter refers to the hazard quotient
of 200 calculated for this scenario.
However, this result was reported as an
intermediate step in the risk assessment
process. EPA had significant concerns
about this result for two basic reasons.
First, this scenario involved storage of
solvent wastes pending incineration.
Modeling limitations required the
Agency to estimate risks based on
solvent storage in tanks without covers
of any kind. In fact, the scenario
assumed that essentially all of the stored
acetonitrile would volatilize from the
tanks before incineration could take
place. The Agency judged this scenario
highly unlikely because the waste is
being stored for thermal treatment, and
it is irrational to assume valuable fuels
would be allowed to escape in such a
manner. Further, as explained in the
proposed rule, the vast majority of the
wastes are already classified as
hazardous waste because they are either
characteristically hazardous, or co-
managed with listed hazardous wastes.
As such, the storage units would have
to comply with RCRA regulations

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            Federal Register/Vol. 63, No. 223/Thursday, November  19,  1998/Rules  and Regulations    64395
 promulgated to control such air releases
 (see 40 CFR part 264, subpart CC). Thus,
 the HQ of 200 is clearly an overestimate,
 because it was based on modeling
 releases for wastes that are already
 hazardous.
   In order to assess potential risks from
 the nonhazardous wastes that were not
 already subject to Subtitle C controls,
 the Agency refocused the assessment on
 the nonregulated waste streams in this
 scenario (acetohitrile in storage tanks).
 This third phase of the risk assessment,
 is a normal and logical step in the
 iterative risk assessment process. Phase
 III of the assessment showed that a
 bounding analysis of these wastes
 resulted in an HQ below one. Therefore,
 EPA concluded that the risks from the
 nonhazardous portion of the acetonitrile
 wastes are not significant, and that
 listing of solvent wastes from the use of
 acetonitrile is not warranted.
   One commenter states that large
 quantities of acetonitrile wastes are
 generated in concentrations well in
 excess of levels capable of posing a
 substantial risk to human health or the
 environment, and are managed in ways
 inconsistent with the Congressional
 directive to minimize the toxicity of
 mobility of wastes destined for  land
 disposal. The commenter stated that
 large quantities of solids containing
 10,000 ppm solvent are disposed in
 hazardous waste landfills, while the
 Universal Treatment Standard (UTS)
 applicable to acetonitrile is 1.8  ppm.
  EPA disagrees that large quantities are
 generated that present substantial risks.
 The Agency evaluated risks based on
 potential exposures arising from
 plausible management. The highest
 concentration of acetonitrile going into
 a surface impoundment is no higher
 than 0.04 mg/L (see Listing Background
 Document, Table 3-2). In fact, it would
 likely be much lower, since those
 wastewaters are pretreated before
 entering the impoundment. As
 described in section IV.C.1, further
 modeling done for surface
 impoundments confirmed that risks
 from such levels were not significant.
  The  commenter is incorrect in stating
 that large quantities of solids containing
 10,000 ppm acetonitrile are disposed in
 hazardous waste landfills.,First, as
 noted previously, very few acetonitrile
 wastes were sent to landfills, i.e., four
 out of the 254 wastes reported in the
 Survey. The commenter singled out the
 one waste with appreciable acetonitrile
loading (454 kg/yr.). In EPA's view, this
one waste is not reflective of "large
quantities" going to landfills.
Furthermore, as described further in the
following response, the practice is no
longer  occurring, and the facility in
 question is currently sending this waste
 stream for fuel blending, in recognition
 of its fuel value.       ,»
   The Agency disagrees with the
 commenter's conclusion that current
 management practices are inconsistent
 with the Congressional directive to
 minimize the toxicity and mobility of
 wastes destined for land disposal. The
 vast majority of the acetonitrile waste
 (nonwastewater), both by volume (99%)
 and by acetonitrile loading (99%), is not
 managed in land-based units.
 Furthermore, as noted above, the vast
 majority of acetonitrile wastes are
 already hazardous, and as such, must
 meet the Land Disposal Treatment
 standards prior to land disposal.
   Finally, as described earlier in today's
 document, some commenters argued
 that EPA should examine more land
 disposal scenarios, such as landfills. In
 response, the Agency examined
 groundwater ingestion risks from the
 disposal of acetonitrile solids in an
 unlined landfill. The Agency still
 believes that landfill disposal of
 acetonitrile is not a plausible
 management scenario, and there is no
 evidence that such waste has ever been
 disposed in Subtitle D landfills. To the
 contrary, the only facility that had been
 sending a significant acetonitrile
 loading to a landfill (454 kg/yr) sent the
 waste to a Subtitle C landfill.
 Furthermore the facility indicated that  it
 had ceased this practice during 1993
 and started sending the waste for
 thermal treatment because of the waste's
 fuel value. (EPA has received
 confirmation from the generator of this
 waste that the material has fuel value on
 the order of 14,800 BTU per pound.1)
 Thus, EPA believes that such wastes
 will be sent for thermal treatment under
 the current regulatory structure. The
 Agency decided, however, to examine
 the resulting risks if such disposal were
 to occur in an unlined Subtitle D
 landfill. As described in more detail in
 the Supplemental Risk Assessment, the
 resulting analysis suggested hazard
 quotients in the range of 11-22 for a
 high-end scenario.
  EPA does not view these risks as
 significant, however, for several reasons.
 First, as noted above, landfill disposal is
 unlikely given the fuel value of the
 material, thus EPA does not view
 disposal in a D landfill plausible. In any
event, the elevated HQs were projected
for only one waste out of the 254
acetonitrile wastes identified in the
3007 Survey. Even if EPA found that the
  1 See contact report dated June 10. 1998
documenting a telephone conversation with Dave
Giffen. B.F. Goodrich, which is located in the
docket accompanying today's rule.
 elevated HQs reflected a plausible
 management scenario, the Agency might
 well decide that the potential risk posed
 by this one waste does not merit listing
 of all acetonitrile residuals generated.
 Given the widely varying nature of the
 industries and wastes involved, and the
 very small percentage of management
 activities that even arguably could
 present a risk of concern, the Agency
 believes that a broad listing for solvent
 use would result in over regulation. In
 any case, EPA concludes that wastes
 such as these are not likely to be
 disposed in landfills, and are therefore
 unlikely to pose significant risks.
   Phenol. Decision. EPA is not listing
 wastes from the solvent use of phenol as
 hazardous waste under 40 CFR 261.31.
 As described in the proposed rule and
 as modified by subsequent analysis in
 response to comments, EPA finds no
 significant risks from treatment in
 aerated tanks, storage in tanks, or
 combustion in a boiler. Furthermore,
 EPA does not believe that potential risks
 from land-based management of phenol
 wastes are significant. None of the
 wastes containing phenol were reported
 to go to landfills. Wastes with high
 organic content that contain any
 appreciable levels of phenol were
 classified as hazardous waste, and were
 sent for fuel blending or incineration as
 hazardous. Wastewaters were generated
 from the specialized use of phenol as a
 solvent in the extraction of materials
 from crude oil, and the resulting spent
 phenol wastes were sent to wastewater
 treatment systems for treatment in tanks
 or surface impoundments. EPA found
 risks from impoundments would be low
 given the dilution and treatment that
 occurs in these wastewater treatment
 systems, and the specific facts
 associated with the impoundment of
 potential concern (see 61 FR 42337).
   In response to comments, EPA
 conducted further analyses of the
 potential risks that might arise from
 treatment of phenol wastewaters in a
 surface impoundment. In these analyses
 EPA also included consideration of any
 additional risk resulting from
 noningestion exposure from
 groundwater (e.g., inhalation), as well as
 codisposal with other solvent wastes
 under evaluation. As described in
 section IV.C, these analyses further
 confirmed this management practice
 presents no significant risks. EPA used
 the updated toxicological benchmark
 discussed in section III of today's rule
for all additional analyses. The Agency
also used the updated toxicological
benchmark to revise the risk assessment
results for other practices, i.e., storage
and treatment in tanks, and found this

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64396    Federal Register/Vol. 63, No. 223/Thursday, November 19, 1998/Rules and Regulations
had no significant impact on the risks
(see Table 3).
  Based the results of the risk analyses
in the proposal, as well as the updated
evaluations, these spent solvent
residuals are not likely to pose a
significant hazard to human health or
the environment. Therefore, the Agency
continues to believe that a no-list
decision is warranted.
  Specific comments. One commenter
supported EPA's decision not to list
wastes from solvent uses of phenol as
hazardous wastes. The commenter
agrees with EPA that phenol does not
satisfy the criteria for listing in 40 CFR
261.11 (a) (3). However, another
commenter stated that there are cases
where phenol is currently used by itself
(without being mixed with other F-
listed wastes) as an industrial solvent
and with this decision "not to list"
phenol as a hazardous waste, EPA
would seem to provide disposal option
"carte blanche" for current users.
Manufacturers can modify their
processes to use these solvents, which
would no longer be considered
hazardous wastes, according to this
commenter.
  In response, the Agency believes it
unlikely that facilities would change
their management practices based on
the information collected in the Survey.
The  Survey indicated that all
nonvvastewater residuals containing
phenol were managed as hazardous
except one, which is managed by
incineration. Thus, the solvent users
managed their wastes as hazardous
under the existing regulatory
framework. There is no evidence that
any facility that has not modified their
process to use these solvents to date will
do so after a no-list decision. Except for
the facilities that use phenol for
extracting lube oil, most facilities that
use phenol as a solvent use it in
laboratories or other specialty uses, and
the waste solvents are sent for offsite
treatment via incineration as hazardous
waste. EPA has no indication that such
generators could easily modify their use
and  accumulation practices in an
attempt to generate nonhazardous
material, nor is there any indication that
facilities would do so.
  A  third commenter stated that EPA's
decisions regarding plausible
mismanagement scenarios are especially
suspect in the case of phenol, because
phenol is the 33rd highest volume
chemical produced in the United States,
is already widely used, and its use is
projected to increase. The commenter
stated that EPA did not adequately
evaluate groundwater risks posed by
phenol.
  EPA disagrees with the commenter's
inference that projected production
increases in phenol are destined for
solvent use. In fact, more than 96% of
the phenol consumed in the U.S. is for
nonsolvent uses (see SRI Chemical
Economics Handbook, 1996). Increasing
demand for products produced from
phenol is due to increases for
production of caprolactam, aniline, and
bisphenol-A, (e.g., see http.7/
www.chemicalweek.com/marketplace/
prod	focus.html). Nearly all of the
solvent use of this chemical (>99.9%)
was attributed to the petroleum
industry, of which the Agency
conducted a complete survey. Given
that the major uses of this solvent were
very specialized (i.e., extraction of lube
oil), the Agency is confident that no
other significant uses are likely to exist.
Contrary to the comment, damage from
groundwater contamination was
evaluated for the proposed rule, and a
refined assessment was conducted for
the final rule, and noted in section IV.B.
These analyses did not find significant
groundwater risks (see Table 2), and
details are given in the Supplemental
Risk Assessment document in the
docket.
  The commenter also noted that EPA's
Hazardous Waste Characteristic Scoping
Study (November 1996) showed that
phenol releases originated from
nonhazardous waste management units,
principally landfills and surface
impoundments. The Scoping Study,
which expressly excluded product spills
and accident releases, presents clear
evidence of the potential risks posed by
the improper management of phenol
wastes, and the use of nonhazardous
surface impoundments and landfills as
plausible mismanagement scenarios for
phenol and other solvent wastes. The
commenter went on to state that EPA
assumed tanks never leak, and landfills
would never be used, because none
were reported by the 31 facilities
receiving the final questionnaire.
  The Agency disagrees that this aspect
of the Characteristic Scoping Study is
relevant to the Solvents Listing
Determination. As EPA noted in the
proposed rule, damage cases reviewed
did not show evidence linking the
phenol contamination at damage sites,
including nonhazardous landfills and
surface impoundments, to phenol use as
a solvent. Without evidence that the
mismanagement of phenol wastes
resulting in contamination is linked to
solvent use, the damage incidents are
not an adequate basis for listing phenol
as a spent solvent. As noted above, the
vast majority of phenol is used for
nonsolvent uses. Therefore simply
pointing to damage case analyses is not
compelling evidence for listing phenol
wastes that result only from its use as
a solvent. If EPA were to determine that
certain industries that use phenol for
nonsolvent uses are mismanaging
wastes and causing significant
environmental problems, then the
Agency would consider other regulatory
approaches. However, EPA's
examination of the limited solvent use
of this chemical indicates that such uses
are not likely ttrgenerate wastes of
concern. Thus, a listing of spent solvent
wastes for this chemical would not be
a practical way to address the types of
environmental concerns raised by the
commenter.
  EPA responded to the general issues
of tanks and landfill disposal elsewhere
in today's document. In the case of
phenol, the Agency did not consider the
disposal of phenol-containing
wastestreams in a landfill to be a
plausible management scenario for
several reasons. None of the 38
wastestreams containing spent phenol
reported in the 3007 Survey are
managed in a landfill. One reason for
this is that very few phenol wastes are
solids (most are organic or aqueous
liquids). Only one solid wastestream,
spent carbon, contained significant
levels of phenol. This was sent offsite
for regeneration or incineration. EPA
has no reason to conclude that the
practice of landfilling will increase.
Wastes with higher organic content are
thermally treated, and 92% of the
thermal treatment was conducted in
hazardous waste units or through fuel
blending for future burning. Therefore,
EPA has no basis to project that wastes
with significant phenol concentration
are likely to be placed in a landfill.
  Methyl Chloride. Decision. EPA is not
listing wastes from the solvent use of
methyl chloride as hazardous waste
under 40 CFR 261.31. As described in
the proposed rule and as modified by
subsequent analysis in response to
comments, EPA finds treatment in
aerated tanks and surface
impoundments, storage in tanks,  or
combustion in a boiler do not  present
significant risk. The vast majority of
methyl chloride produced is used as an
intermediate in chemical
manufacturing, and very few uses as a
solvent were identified. Essentially all
of the wastes reported from the solvent
uses of methyl chloride were limited to
two facilities that produce butyl rubber.
While some of the updated lifetime
individual excess cancer risks in  Table
3 for storage in tanks and wastewater
treatment in tanks/surface
impoundments were above 1E-06, the
risks are below the  IE-OS level typically
used by the Agency for identifying

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           Federal Register/Vol. 63. No. 223/Thursday, November  19,  1998/Rules and Regulations     64397
 candidate wastes for listing.
 Furthermore, as described below, the
 consideration of other factors indicate
 these risks are not significant.
   The high-end risks for storage tanks
 (4E-06 from the updated analysis and
 2E-06 from the Air Characteristic
 approach) are highly likely to be
 overestimates, because the analyses
 assumed that all of the methyl chloride
 in the stored solvent waste would be
 released. This assumption is unlikely
 for materials being stored expressly to
 send for thermal treatment.
 Furthermore, these wastes were
 reported to be already regulated as
 hazardous, and would be subject to
 RCRA regulations limiting air releases
 under 40 CFR part 264, subpart CC.
   The risks found for wastewater
 treatment tanks (1E-06 from the
 updated analysis, and 1E-07 from the
 Air Characteristic approach) are at or
 below EPA's presumptive no-list level
 of 1E-06, and do not appear of concern.
 In addition, these are likely to be
 overestimates, because the
 concentration modeled for this scenario
 was 10 ppm, even though the value was
 actually reported as less than 10 ppm.
 EPA's updated assessment of the one
 wastewater reported to be treated in a
 surface impoundment showed a high-
 end risk of 4E-06. However the one
 impoundment that managed this waste
 is already a permitted Subtitle C
 hazardous waste unit, and is therefore
 subject to regulations limiting air
 releases (see 40 CFR part 264, subpart
 CC) and groundwater release ( 40 CFR
 part 264, subparts F and K,).
   In addition, potential air releases from
 this industry are being addressed by
 other regulations promulgated under the
 Clean Air Act (see 61 FR 46906,
 September 5, 1996). These regulations
 control releases of hazardous air
 pollutants from process units, storage
 tanks and wastewater treatment
 systems. EPA believes that these air
 regulations provide a more integrated
 approach to controlling air risks than
 would be possible under the limited
 controls available for air releases under
 the RCRA listing program.
  Based on the analysis in the proposal,
 the updated evaluations, and the other
 factors discussed in this document and
 the proposal, the methyl chloride
 solvent wastes are not likely to pose a
significant hazard to human health or
the environment. Therefore, the Agency
 continues to believe that a no-list
 decision is warranted.
  Specific Comments. One commenter
supported the Agency's decision not to
list methyl chloride. However, another
commenter stated that the Agency left
potential risks posed by the
 groundwater exposure pathway
 unevaluated by assuming methyl
 chloride was managed only in a
 permitted surface impoundment, that
 tanks never leak, and that landfills
 would never be used.
   As discussed more detail in the
 proposed rule (see 61 FR at 42334-
 42335), the Agency did evaluate the
 groundwater exposure pathway through
 management scenarios where
 groundwater exposure was plausible.
 Wastes with high organic content were
 regulated as hazardous and incinerated.
 Waste solids were rarely sent to
 landfills, and in these cases the
 concentrations of methyl chloride were
 negligible. The only wastes sent to
 landfills were a small volume of spent
 desiccant that contained <5 kg of methyl
 chloride, and a larger volume sludge/
 ash from a sludge treatment unit which
 was reported to have a "trace" amount
 of methyl chloride. Given that this
 chemical is readily treated by
 biodegradation and volatilization in an
 aerated biological treatment system, it is
 unlikely that any significant levels of
 methyl chloride remain in this residual.
 EPA believes that these very low
 concentration wastes reflect the types of
 waste solids that are likely to be sent to
 landfills. EPA also notes that other
 nonwastewaters containing any reported
 levels of methyl chloride (a total loading
 of 1.6 kg) were regulated as hazardous
 waste, making disposal in an unlined
 Subtitle D landfill illegal. Thus,
 significant groundwater risks from
 landfills are unlikely to occur.
   The very limited solvent use of this
 chemical, and its unique characteristics
 (a gas at room temperature) lead EPA to
 conclude that it is unlikely that other
 solvent wastes would be generated that
 are managed in other surface
 impoundments beyond the example
 documented in the 3007 survey. As
 noted above, this impoundment is a
 hazardous waste unit, and is therefore
 subject to RCRA regulations limiting
 groundwater releases. Furthermore, as
 noted in the proposed rule, methyl
 chloride is readily treated by
 biodegradation and volatilization in
 waste water treatment systems, and thus
 is unlikely to migrate to the
 groundwater. Also, the tendency of
 methyl chloride to hydrolyze in water to
 methanol suggests that transport to
 receptors by groundwater is not likely to
 be significant.
  One commenter argued that EPA
 failed to adequately consider the
formation of products of incomplete
 combustion (PICs) for methyl chloride.
The commenter stated that EPA claimed
PIC emissions were not cause for
concern because the reported waste in
 question happened to be managed in a
 hazardous waste combustor, and
 disagreed with EPA's presumption that
 this one waste management practice
 reported represents current and future
 combustion activities.
   As noted above, the solvent uses of
 methyl chloride are very specialized,
 and the number of wastes sent for
 incineration are limited. The three
 wastes with reported concentrations
 that went to thermal treatment were all
 classified as hazardous waste and were
 treated as such under RCRA regulations.
 (Two wastes incinerated were treatment
 sludges that were reported to contain no
 significant levels of methyl chloride).
 Given these reported practices, and the
 very limited solvent uses for this
 chemical, EPA believes that combustion
 of solvent wastes with appreciable
 methyl chloride is likely to occur in
 RCRA regulated units. Therefore, the
 Agency believes its presumption for
 management is valid in this case. In
 addition, EPA is not aware of any
 precise way of predicting the kinds or
 levels of PICs that might be generated in
 a nonhazardous boiler, especially
 because the wastes in question would
 make up only a very small fraction of
 the wastes being treated.
   Nevertheless, EPA did consider the
 possibility of PIC formation for
 incineration of methyl chloride wastes.
 As discussed in the preamble to the
 proposed rule  (61 FR 42334), the
 amount of methyl chloride in the wastes
 that are incinerated is extremely small
 (i.e., 2 kg). The loading of methyl
 chloride sent to a boiler or industrial
 furnace (BIF), although larger (i.e., at
 2,250 kg) than the amount sent to an
 incinerator, is in a waste that is
 hazardous due to ignitability and
 toxicity characteristics, and therefore
 must be treated as hazardous wastes.
 This latter waste is generated from the
 use of methyl chloride in butyl rubber
 manufacturing, and it is unlikely that
 such a complex process could (or
 would) be modified to avoid generating
 waste methyl chloride in association
 with high levels of ignitable
 hydrocarbons. Thus, combustion in a
 RCRA-regulated unit seems likely to
 occur for this waste due to the
specialized nature of this solvent use.
These combustion units are operated
according to stringent air emission
standards that limit PIC formation (e.g.,
see 40 CFR part 264, subpart O, for
incinerators and part 266, subpart H, for
Boilers and Industrial Furnaces). EPA
has also proposed revisions to these
standards (see 61FR1538, April 19, 1996
and 62FR24212, May 2, 1997). Given
these facts, as well as the results of the
risk assessment for these wastes, EPA

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64398    Federal Register/Vol. 63, No. 223/Thursday, November 19, 1998/Rules and Regulations
does not believe that combustion of
these wastes poses a significant risk.
  2-Methoxyethanol (2-ME). Decision
EPA is not listing wastes from the
solvent use of 2-methoxyethanol (2-ME)
as hazardous waste under 40 CFR
261.31. As described in the proposed
rule and as modified by subsequent
analysis in response to comments, EPA
found no significant risks from
treatment in aerated tanks or
combustion in a boiler. EPA also
concluded that potential risks from air
releases of 2-ME stored in open
accumulation tanks are also not
significant, because all of the
nonwastewater residuals stored under
this scenario are already regulated as
hazardous waste, either because the
wastes exhibit a characteristic, or
because the 2-ME waste is commingled
with listed wastes. EPA believes that
regulatory controls afforded by the
existing solvent listings and the
characteristics (primarily ignitability)
are sufficiently protective of human
health and the environment.
  None of the wastes examined were
sent to land disposal in a landfill or
impoundment. Spent solvent solids are
thermally treated, and wastewaters are
all treated in tanks. In the face of the
existing practices, EPA finds it
implausible that high organic wastes
currently sent to thermal treatment
would be sent to landfills. Essentially
all of the nonwastewater residuals that
contain spent 2-ME are thermally
treated or recovered, and nearly all
(96%)  are treated as hazardous waste.
Because all wastewaters are treated in
tanks, EPA also does not expect risks
from surface impoundment management
for these wastes.
  Given that nearly all of the
nonwastewater 2-ME residuals are
already being handled as hazardous, or
contain negligible amounts of the
solvent, these spent solvent residuals
are not likely to pose a significant
hazard to human health or the
environment. Furthermore, treatment of
wastewaters in tanks presents no
significant risks. Therefore, the Agency
continues to believe that a no-list
decision is warranted.
  More general comments on EPA's
methodology and approach that relate to
2-ME are discussed elsewhere in
today's document. The few comments
specific to 2-ME are discussed below.
  Specific comments. One commenter
stated that EPA completely failed to
evaluate potential risks from
groundwater contamination,
notwithstanding three groundwater
contamination incidents involving this
solvent identified by EPA from damage
incidents.
  EPA described in the proposed rule
why the damage cases cited by the
commenter were not useful (see 61 FR
at 42332). Of the three problem site
identified, two were old landfills that
received a wide variety of industrial and
municipal wastes, and the use of 2-ME
prior to disposal was impossible to
ascertain. The chemical is widely used
as a fuel additive and as a chemical
intermediate. Thus, the damage could
not be tied to wastes generated from the
use of this chemical as a solvent.
Damage at the third site also could not
be linked to a specific use of 2-ME.
However, this site was a used oil
recycling site, and the contamination
found may be related to the use of 2-
ME as a fuel additive. Furthermore,
none of the reports examined by the
Agency provided any concentration of
2-ME in the groundwater. Thus, the
limited data from the damage incidents
provide no reliable support for listing
wastes from the use of 2-ME as a
solvent. In addition, the industries EPA
identified as solvent users of 2-ME are
not represented in the damage
incidents. Finally, the vast majority of
nonwastewater solvent wastes identified
in the Survey were reported to be
hazardous waste, and could not be
placed in nonhazardous landfills. Thus,
the damage incidents did not provide
useful information on current or likely
future waste management practices.
  One commenter argued that EPA's
high-end risk analysis of onsite
accumulation tank storage resulted in a
HQ of 16, well above the HQ of 1 that
typically warrants a hazardous waste
listing. Only by performing the
completely misguided Phase III
assessment was EPA able to arguably
rationalize a no-list decision.
  EPA's response to this comment is
similar to the response above to
essentially the same comment raised for
acetonitrile. The apparent risks cited by
the commenter were from an
intermediate stage of the risk
assessment, and did not reflect the fact
that all nonwastewaters were managed
as hazardous waste. EPA concluded that
the management scenario referred to in
the comment (on-site accumulation of
nonwastewaters in unregulated tanks)
does not apply to any 2-methoxyethanol
waste streams.
  2-Ethoxyethanol Acetate (2-EEA).
Decision. EPA is not listing wastes from
the solvent use of 2-ethoxyethanol
acetate (2-EEA) as hazardous waste
under 40 CFR 261.31. As described in
the proposed rule and as modified by
subsequent analysis in response to
comments, EPA found no significant
risks  from treatment in aerated tanks,
storage in tanks, or combustion in a
boiler. Furthermore, essentially all
(99.8%) of the nonwastewaters were
reported to be hazardous and were
managed as hazardous waste through
some form of thermal treatment.
  None of the wastes were reported to
go to land disposal in landfills or
impoundments, and these scenarios
were not modeled. Given the existing
waste management practices, EPA finds
it implausible that high organic waste
solids currently sent to thermal
treatment would be sent to a landfill.
The high percentage of wastes that are
hazardous are precluded from disposal
in an unlined Subtitle D landfill, and
EPA has no evidence to indicate that
spent 2-EEA wastes would be placed in
a landfill. Due to the nature of the
primary industries using 2-EEA as a
solvent (e.g., the semiconductor and
electronics industries), very few
wastewaters are generated. Nearly all of
the wastestreams generated are spent
solvent wastes that undergo  some type
of thermal treatment. None of the
wastestreams that  were reported in the
3007 Survey go to a surface
impoundment. Any change from the
current treatment  in tanks to treatment
in impoundments seems unlikely  given
the capital investment associated with
tanks and the liability issues associated
with treatment in  a surface
impoundment. These facilities made an
investment in.tank-based systems in the
absence of any listing, and EPA sees no
reason why this would change if the
status quo is not changed, i.e., if the
wastes are not listed. In addition to cost
considerations, some facilities may
perceive other benefits from managing
the waters in tanks, such as the current
exemption from RCRA permitting
requirement for such units (see 40 CFR
264.1 (g) (6)). If hazardous waste were to
be treated in a wastewater treatment
system, impoundments in the system
would require permitting as a Subtitle C
unit. In addition, the use of 2-EEA has
been decreasing in recent years, thus
other new generators of this spent
solvent are unlikely.
   Given that nearly all of the
nonwastewater 2-EEA residuals are
already being handled as hazardous, or
contain negligible amounts of the
solvent, these spent solvent  residuals
are not likely to pose a significant
hazard to human health or the
environment. Furthermore, treatment of
wastewaters in tanks presents no
significant risks. Therefore, the Agency
continues to believe that a no-list
decision is warranted.
   More general comments on EPA's
methodology and  approach that relate to
2-EEA are discussed elsewhere in
today's document. The few comments

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           Federal Register/Vol. 63, No. 223/Thursday, November 19, 1998/Rules and  Regulations    64399
 related specifically to 2-EEA are
 discussed below.
   Specific comments. Two commenters
 stated that EPA failed to consider in its
 risk assessment, that many of the
 generators manage 2-EEA with other
 solvents associated with this proposed
 rule. EPA calculated an HQ for 2-EEA
 for on-site accumulation of 0.7. Thus,
 additional risk from other solvents
 would cause the HQ level to exceed the
 threshold of one. One of the
 commenters went on to cite examples of
 facilities in several industries (e.g.,
 printed circuit board manufacturers) at
 which multiple solvents were reported.
   EPA disagrees with the commenters'
 concerns about multiple solvent risks.
 First, the comment cited examples
 where the hazard quotient would
 exceed one at facilities that use more
 than one solvent in combination.
 However, the use of the chemicals at the
 facilities cited by the commenter are not
 solvent use, within the Agency's
 definition. These facilities used 2-EEA
 and other chemicals as components in
 formulations. Thus, no spent solvent is
 generated and was not included in the
 risk assessment.
   Furthermore, the HQ value of 0.7
 cited by the commenter for on-site
 accumulation is likely to be
 unrealistically high for the reasons cited
 for the Phase II results for acetonitrile.
 The key reason is that essentially all
 residuals stored prior to thermal
 treatment were, in fact, already
 hazardous waste. Thus, air emissions
 from these wastes are already regulated
 under RCRA subpart CC to 40 CFR part
 264, making the scenario of storage  in
 an open tank unrealistic. EPA did not
 pursue a third phase of analysis for  2-
 EEA because the HQ was below one in
 the Phase II evaluation. Furthermore,
 the only wastes reported that were not
 hazardous consisted of one insignificant
 loading (<1 kg), and one waste
 characterized as "containers/rags"
 which contained very low levels of the  •
 solvent (<6 kg). Thus, EPA decided
further analysis was. not needed. As
 described in the Risk Assessment
 section, EPA addressed the general
 comment of the impact of multiple
solvents in some wastes by conducting
 an assessment of the potential for
 cumulative risks.
  One commenter stated that the
concentrations of 2-EEA in solvent
 nonwastewaters range from 0.1% to
 100%. These ranges are not consistent
with the Agency's position that
nonwastewaters would always be
managed as a hazardous waste due to
ignitability, particularly where the
solvent is not co-managed with listed
solvent wastes. The commenter was also
 concerned because the concentration of
 2-EEA in wastewaters ranges from 200-
 20,000 ppm.
   While the levels of 2-EEA in solvent
 nonwastewaters are variable, the
 reported data clearly indicate that
 essentially all 2-EEA solvent wastes
 generated were hazardous, and that
 these were all incinerated. Concerning
 the wastewaters, EPA believes the
 commenter's concern is unfounded.
 EPA's risk assessment included an
 analysis of potential risks from air
 releases from an aerated wastewater
 treatment tank, and found risks to be
 well below levels of concern.
   Furfural. Decision. EPA is not listing
 wastes from the solvent use of furfural
 as hazardous waste under 40 CFR
 261.31. As described in the proposed
 rule and as modified by subsequent
 analysis in response to comments, EPA
 found no significant risks from
 treatment in aerated tanks or surface
 impoundments, storage in tanks, or
 combustion in boilers. Essentially all of
 the solvent use of this chemical (greater
 than 99.99%) is in the petroleum
 industry as an extractant for lube oil.
 Thus, solvent use of furfural is limited,
 and the Agency identified only a
 handful of wastes derived from this use.
  The furfural solvent wastes are
 virtually all wastewaters  (greater than
 99.99%), which were managed in
 wastewater treatment systems.  One of
 the three facility's wastewater treatment
 systems uses a surface impoundment,
 and EPA's bounding analysis for the
 proposed rule showed no risks of
 concern from ingestion of groundwater,
 or inhalation of possible air releases
 (HQ <1; see 61 FRat 42341).
  In response to comments, EPA
 conducted further analyses of the
 potential risks that might arise from
 treatment of furfural wastewaters in a
 surface impoundment. In these analyses
 EPA also included consideration of any
 additional risk resulting from non-
 ingestion exposure from groundwater
 (e.g., inhalation). As shown in Table 3,
 the high-end risk analyses showed that
 these wastewaters do not present
 significant risks via either groundwater
 releases (HQ = 0.46), or air releases
 (HQ = 0.11).
  Based the results of the risk analyses
 in the proposal, the updated
 evaluations, and the other factors
 discussed in this document and the
 proposal, the furfural solvent wastes are
not likely to pose a significant hazard to
human health or the environment.
Therefore, the Agency continues to
believe that a no-list decision is
warranted.
  General comments on EPA's
methodology and approach that relate to
 furfural are discussed elsewhere in
 today's document. EPA did not receive
 any other specific comments on EPA's
 decision not to list furfural solvent
 wastes.
   Cumene. Decision. EPA is not listing
 wastes from the solvent use of cumene
 as hazardous waste under 40 CFR
 261.31. As described in the proposed
 rule and as modified by subsequent
 analysis in response to comments, EPA
 found no significant risks from
 treatment in aerated tanks, storage in
 tanks, or combustion in boilers. While
 cumene is used in large volumes in the
 production of other chemicals, such as
 phenol, its use  as a solvent is limited.
 Essentially all of the wastes containing
 cumene are thermally treated as
 hazardous or recovered. Small amounts
 of wastewaters  are sent to treatment
 systems, and one  resulting sludge was
 reported to be landfilled.  However, the
 amount of cumene in this sludge would
 be well below the maximum of 28 kg
 that was used in the original solvent
 mixture (which contained only 1.7 % of
 cumene to start with). Thus, after
 treatment, any risks from cumene would
 be negligible. Similarly, one wastewater
 was reported to undergo treatment in a
 surface impoundment, however, as EPA
 noted in the proposal, the amount of
 cumene in the wastewater was small
 (<47 kg), and would be further reduced
 by treatment.
   In response to comments, EPA
 conducted further analyses of the
 potential risks that might arise from
 treatment of cumene wastewaters in  a
 surface impoundment. In these analyses
 EPA also included consideration of any
 additional risk resulting from non-
 ingestion exposure from groundwater
 (e.g., inhalation during showering). As
 shown in Table 2, the revised bounding
 analyses showed that these wastewaters
 in impoundments do not present
 significant risks via either groundwater
 releases (HQ = 0.0001), or air releases
 (HQ = 0.003). As noted earlier in today's
 document, the toxicological values for
 cumene were updated during the
 comment period. The new benchmarks
were used in the revised analyses, and
were also used to  recalculate risks
 derived in the proposed rule (see Table
 1). The changes reflect greater tolerance
for cumene than the previous
benchmarks, and thus have no impact
on EPA's decision not to list cumene
solvent wastes.
  EPA also considered the potential for
cumene to form NAPLs, which might
present special problems in assessing
potential risks. EPA noted in the
proposed rule that cumene's water
solubility is relatively low, such that
NAPLs are theoretically possible.

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64400    Federal Register/Vol.  63,  No. 223/Thursday, November 19, 1998/Rules and Regulations
However, EPA considered the potential
risks from NAPLs to be very low,
because cumene loading in wastes sent
to land-based disposal was minimal. In
response to comments, EPA provided
further analysis showing that NAPL
formation for these wastes is unlikely
(see section IV.B).
  Based the results of the risk analyses
in the proposal, the updated
evaluations, and the other factors
discussed in this document and the
proposal, the cumene solvent wastes are
not likely to pose a significant hazard to
human health or the environment.
Therefore, the Agency continues to
believe that a no-list decision is
warranted.
  General comments on EPA's
methodology and approach that relate to
cumene are discussed elsewhere in
today's document.
  Cyclohexanol. Decision. EPA is not
listing wastes from the solvent use of
cyclohexanol as hazardous waste under
40 CFR 261.31'. As described in the
proposed rule and as modified by
subsequent analysis in response to
comments, EPA found no significant
risks from accumulation in storage in
tanks or combustion in boilers. The
solvent uses of cyclohexanol are
limited, and few wastes containing
cyclohexanol were reported. All wastes
but one are hazardous waste due to
other waste constituents or properties of
the waste material. The incinerated
material contains low levels of
cyclohexanol (16 kg total loading per
year). The one other waste generated
was reported to go to a nonhazardous
landfill, however, this waste is a small
volume (750 kg) of filter material that
contains negligible level of
cyclohexanol. Given the  limited solvent
uses of this chemical, and the
management practices reported, EPA
believes other wastes or management
practices are not likely to be significant.
  As noted earlier in today's document,
the toxicological inhalation benchmark
("provisional RfC") for cyclohexanol
was adjusted somewhat based on peer
review comments. Thus, EPA used the
new benchmark to  recalculate risks
derived in the proposed rule (see Table
3). The revised HQs remain below one,
and thus the updated health-based
number has no material effect on EPA's
decision not to list cyclohexanol solvent
wastes.
  Based the results of the risk analyses
in the proposal, the updated
evaluations, and the other factors
discussed in this document and the
proposal, the cyclohexanol solvent
wastes are not likely to pose a
significant hazard to human health or
the environment. Therefore, the Agency
continues to believe that a no-list
decision is warranted.
  More general comments on EPA's
methodology and approach that relate to
cyclohexanol are discussed elsewhere in
today's document.
  Isophorone. Decision. EPA is not
listing wastes from the solvent use of
isophorone as hazardous waste under 40
CFR 261.31. As described in the
proposed rule and as modified by
subsequent analysis in response to
comments, EPA found no significant
risks from accumulation in storage in
tanks or combustion in boilers. The
solvent uses of isophorone are limited,
and few wastes containing isophorone
were reported. All wastes but one were
hazardous waste due to mixture with
other listed wastes or the ignitability
characteristic of the waste material. All
wastes were reported to undergo some
form of thermal treatment as a
hazardous waste. Given the limited
solvent uses of this chemical, and the
management practices reported, EPA
believes other wastes or management
practices are likely to be significant.
  As noted earlier in today's document,
the toxicological value ("provisional
RfC") for isophorone was adjusted
somewhat based on peer review
comments. Thus, EPA used the new
benchmark to recalculate risks derived
in the proposed rule (see Table 1). The
revised HQs remain below one, and thus
the updated health-based number has
no material effect on EPA's decision not
to list isophorone solvent wastes.
  Based on the results of the risk
analyses in the proposal, the updated
evaluations, and the other factors
discussed in this document and the
proposal, the isophorone solvent wastes
are not likely to pose a significant
hazard to human health or the
environment. Therefore, the Agency
continues to believe that a no-list
decision is warranted.
  More general comments on EPA's
methodology and approach that relate to
isophorone are discussed elsewhere in
today's document.
  2-Methoxyethanol Acetate (2-MEA).
Decision. EPA is not listing wastes from
the solvent use of 2-methoxyethanol
acetate (2-MEA) as hazardous waste
under 40 CFR 261.31. As described in
the proposed rule and as modified by
subsequent analysis in response to
comments, EPA found no significant
risks from storage in tanks or
combustion in a boiler. 2-MEA is
reportedly no longer produced
domestically, and solvent use of this
chemical is limited. The few wastes
generated were classified as hazardous
and were all thermally treated as
hazardous waste. Given the limited and
decreasing use as a solvent, and the
waste information reported, EPA
believes that other wastes and
management practices are unlikely.
None of the wastes were reported to be
disposed of in landfills or
impoundments, and these scenarios
were not modeled.
  Given the existing practice, EPA finds
it implausible that high organic waste
solids currently sent to thermal
treatment would be sent to a landfill.
The wastes are hazardous and thus
precluded from disposal in an unlined
Subtitle D landfill.  EPA has no evidence
to indicate that spent 2-MEA wastes
would be placed in a landfill. Due to the
nature of the solvent uses reported for
2-MEA (diluent in coating and reaction
media), no wastewaters are generated,
nor were they expected.
  Based on the results of the risk
analyses in the proposal, the updated
risk analysis,  and other factors noted
above and in the proposed rule, these
spent solvent residuals are not likely to
pose a significant hazard to human
health or the environment. Therefore,
the Agency continues to believe that a
no-list decision is warranted.
  More general comments on EPA's
methodology  and approach that relate to
isophorone are discussed elsewhere in
today's document. EPA did not receive
any specific comments on EPA's
decision not to list  2-MEA solvent
wastes.
  Chemicals with no significant solvent
use. As described in the proposed rule
and reaffirmed in this final decision,
EPA did not find any significant solvent
use for four chemicals: p-
dichlorobenzene, benzyl chloride,
epichlorohydrin, and ethylene
dibromide. All but  one are relatively
reactive chemicals, which makes them
unsuitable for most solvent
applications. The other substance, p-
dichlorobenzene, is a solid at room
temperature, limiting its utility as a
solvent. In all cases, the data collected
by the Agency showed that any solvent
use of these chemicals is extremely
limited. Some may perhaps have
specialty applications in laboratories,
but no significant solvent uses were
identified. Any residuals reported from
the 3007 Survey were primarily from
possible solvent use by laboratories and
contain low levels of the chemicals
under study. All were coded as
hazardous, except one dilute
wastewater, and were thermally treated
as hazardous waste.
  The Agency received no new
information during the comment period
indicating that these four chemicals,
(benzyl chloride, epichlorohydrin,
ethylene dibromide, and p-

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            Federal Register/Vol.  63,  No. 223/Thursday, November  19,  1998/Rules and Regulations     64401
 dichlorobenzene) were used as solvents.
 Comments received by EPA on this
 issue concurred with the Agency's
 decision that these four chemicals are
 not used as solvents, and that they
 would not fit the description for such a
 listing. Based on the analyses and
 factors noted above and in the proposed
 rule, these spent solvent residuals do
 not pose a significant hazard to human
 health or the environment. Therefore,
 the Agency continues to believe that no-
 list decisions for these four chemicals
 are warranted.

 V. Regulatory Requirements

 A. Regulatory Impact Analysis Pursuant
 to Executive Order 12866
   Executive Order No. 12866 requires
 agencies to determine whether a
 regulatory action is "significant." The
 Order defines a "significant" regulatory
 action as one that "is likely to result in
 a rule that may: (1) have an annual
 effect on the economy of $100 million
 or more or adversely affect, in a material
 way, the economy, a sector of the
 economy,  productivity, competition,
 jobs, the environment, public health or
 safety, or State, local, or tribal
 governments or communities;  (2) create
 serious inconsistency or otherwise
 interfere with an action taken or
 planned by another agency; (3)
 materially  alter the budgetary impact of
 entitlements, grants, user fees, or loan
 programs or the rights and obligations of
 recipients; or (4) raise novel legal or
 policy issues arising out of legal
 mandates,  the President's priorities, of
 the principles set forth in the Executive
 Order."
  The Agency estimated the costs of
 today's final rule to determine if it is a
 significant regulation as defined by the
 Executive Order. Because the Agency
 has decided not to list as hazardous the
 wastes generated from the use of the
 solvents evaluated in this rulemaking,
 no specific action is required under this
 action. As a result, there are no costs
 associated  with this final rule. This rule
 was deemed significant for novel policy
 reasons by  the Office of Management
 and Budget (OMB) and was submitted to
 OMB for review.

 B. Regulatory Flexibility 'Act
  Pursuant to the Regulatory Flexibility
 Act (5 U.S.C. 601 et seq., as amended by
 the Small Business Regulatory
 Enforcement Fairness Act (SBREFA) of
 1996) whenever an agency is required to
 publish a document of rulemaking for
 any proposed or final rule, it must
prepare and make available for public
comment a regulatory flexibility
analysis that describes the effect of the
 rule on small entities (i.e., small
 businesses, small organizations, and
 small governmental jurisdictions).
 However, no regulatory flexibility
 analysis is required if the head of an
 agency certifies the rule will not have a
 significant economic impact on a
 substantial number of small entities.
   SBREFA amended the Regulatory
 Flexibility Act to require Federal
 agencies to provide a statement of the
 factual basis for certifying that a rule
 will not have a significant economic
 impact on a substantial number of small
 entities. The following discussion
 explains EPA's determination. This rule
 has no effect as the Agency is issuing
 this final decision not to list wastes
 generated from the use of 14 chemicals
 as solvents as hazardous under the
 Resource Conservation and Recovery
 Act (RCRA). The determinations in this
 rule are limited to specific solvent
 wastes. The rule does not impose new
 burdens on small entities. Therefore, I
 hereby certify that this rule will not
 have a significant economic impact on
 a substantial number of small entities.
 This rule, therefore, does not require a
 regulatory flexibility analysis.

 C. Unfunded Mandates Reform Act
   Title II of the Unfunded Mandates
 Reform Act of 1995 (UMRA), Public
 Law No. 104-4, establishes
 requirements for Federal agencies to
 assess the effects of their regulatory
 actions on State, local, and tribal
 governments and the private sector.
 Under section 202 of the UMRA, EPA
 generally must prepare a written
 statement, including a cost-benefit
 analysis, for proposed and final rules
 with Federal mandates that may result
 in expenditures to State, local, and
 tribal governments, in the aggregate, or
 to the private sector, of $100 million or
 more in any one year. Before
 promulgating an EPA rule for which a
 written statement is needed, section 205
 of the UMRA generally requires EPA to
 identify and consider a reasonable
 number of regulatory alternatives and
 adopt the least costly, most cost-
 effective, or least burdensome
 alternative that achieves the objectives
 of the rule. The provisions of section
 205 do not apply when they are
 inconsistent with applicable law.
 Moreover, section 205 allows EPA to
 adopt an alternative other than the least
 costly, most cost-effective, or least
 burdensome alternative if the
Administrator publishes with the final
rule an explanation why that alternative
was not adopted. Before EPA establishes
any regulatory requirements that may
significantly or uniquely affect small
governments, including tribal
 governments, it must have developed
 under section 203 of the UMRA a small
 government agency plan. The plan must
 provide for notifying potentially
 affected small governments, enabling
 officials of affected small governments
 to have meaningful and timely input in
 the development of EPA regulatory
 proposals with  significant Federal
 intergovernmental mandates, and
 informing, educating, and advising
 small governments on compliance with
 the regulatory requirements.
   EPA has determined that this rule
 does not include a Federal mandate that
 may result in estimated costs of $100
 million or more to either State, local, or
 tribal governments in the aggregate. The
 rule would not  impose any federal
 intergovernmental mandate because it
 imposes no enforceable duty upon State,
 tribal or local governments.  States,
 tribes and local governments have no
 compliance costs under this rule. For
 the same reasons, EPA also has
 determined that this rule contains no
 regulatory requirements that might
 significantly or  uniquely affect small
 governments. In addition, as discussed
 above, the private sector is not expected
 to incur costs exceeding $100 million.
 By these findings, EPA has fulfilled the
 requirement for analysis under the
 Unfunded Mandates Reform Act.

 D. Executive Order 12875: Enhancing
 the Intergovernmental Partnership
  Under Executive Order  12875, EPA
 may not issue a  regulation that is not
 required by statute and that creates a
 mandate upon a State, local or tribal
 government, unless the Federal
 government provides the funds
 necessary to pay the direct compliance
 costs incurred by those governments, or
 EPA consults with those governments. If
 EPA complies by consulting. Executive
 Order  12875 requires EPA to provide to
 the Office of Management and Budget a
 description of the extent of EPA's prior
 consultation with representatives of
 affected State, local and tribal
 governments, the nature of their
 concerns, copies of any written
 communications from the governments,
 and a statement  supporting the need to
 issue the regulation. In addition,
 Executive Order 12875 requires EPA to
 develop an effective process permitting
 elected officials  and other
 representatives of State, local and tribal
 governments "to provide meaningful
 and timely input in the development of
regulatory proposals containing
significant unfunded mandates."
  Today's rule does not create a
mandate on State, local or tribal
governments. The rule does not impose
any enforceable duties on these entities.

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64402    Federal Register/Vol. 63, No.  223/Thursday,  November 19, 1998/Rules  and Regulations
It issues a final decision not to list
wastes generated from the use of 14
chemicals as solvents as hazardous
under the Resource Conservation and
Recovery Act (RCRA). Accordingly, the
requirements of section l(a) of
Executive Order 12875 do not apply to
this rule.
E. Executive Order 13045: Protection of
Children From Environmental Health
Risks and Safety Risks
  Executive Order 13045: "Protection of
Children from Environmental Health
Risks and Safety Risks" (62 FR  19885,
April 23, 1997) applies to any rule that:
(1) is determined to be "economically
significant" as defined under E.O.
12866, and (2) concerns an
environmental health or safety risk that
EPA has reason to believe may have a
disproportionate effect on children. If
the regulatory action meets both criteria,
the Agency must evaluate the
environmental health or safety effects of
the planned rule on children, and
explain why the planned regulation is
preferable to other potentially effective
and reasonably feasible alternatives
considered by the Agency.
  This final rule is not subject to the
Executive Order because it is not
economically significant as defined in
E.O. 12866, and because the Agency
does not have reason to believe the
environmental health or safety risks
addressed by this action present a
disproportionate risk to children. The
Agency performed a risk assessment to
assist in its determination whether to
list or not to list the solvent wastes in
this final rule as hazardous waste.  This
risk assessment calculated the potential
risk resulting from the current
management of these wastes to
individuals (including sensitive
populations like children). The Agency
has determined that management of
these solvent wastes as hazardous  is not
required and that the environmental
health risks or safety risks addressed by
this action do not have a
disproportionate effect on children.
F. Environmental Justice E.O. 12898
  EPA is committed to addressing
environmental justice concerns and is
assuming a leadership role in
environmental justice initiatives to
enhance environmental quality for all
residents of the United States. The
Agency's goals are to ensure that no
segment of the population, regardless of
race, color, national origin, or income
bears disproportionately high and
adverse human health and
environmental impacts as a result of
EPA's policies, programs, and activities,
and that all people live in clean and
sustainable communities. In response to
Executive Order 12898 and to concerns
voiced by many groups outside the
Agency, EPA's Office of Solid Waste
and Emergency Response formed an
Environmental Justice Task Force to
analyze the array of environmental
justice issues specific to waste programs
and to develop an overall strategy to
identify and address these issues
(OSWER Directive No. 9200.3-17). The
Agency has determined that a hazardous
waste listing is not justified for the
wastes examined in this rule. As a
result, no specific action is required
under this rule. It is, therefore, not
expected to result in any
disproportionately negative impacts on
minority or low income communities
relative to affluent or non-minority
communities.

G. Paperwork Reduction Act
  This rule does not contain any
information collection requirements
subject to OMB review under the
Paperwork Reduction Act of 1980, 44
U.S.C. 3501  etseq.
H. National Technology Transfer and
Advancement Act
  Section 12(d) of the National
Technology Transfer and Advancement
Act of 1995  ("NTTAA"), Pub L. No.
104-113, §12(d) (15 U.S.C. 272 note)
directs EPA to use voluntary consensus
standards in its regulatory activities
unless to do so would be inconsistent
with  applicable law or otherwise
impractical. Voluntary consensus
standards are technical standards (e.g.,
materials specifications, test methods,
sampling procedures, and business
practices) that are developed or adopted
by voluntary consensus standards
bodies. The NTTAA directs EPA to
provide Congress, through OMB,
explanations when the Agency decides
not to use available and applicable
voluntary consensus standards. This
action does  not involved technical
standards. Therefore, EPA did not
consider the use of any voluntary
consensus standards.

L Executive Order 13084: Consultation
and Coordination With Indian Tribal
Governments
   Under Executive Order 13084, EPA
may not issue a regulation that is not
required by statute, that significantly or
uniquely affects the communities of
Indian tribal governments, and that
imposes substantial direct compliance
costs on those communities, unless the
Federal government provides the funds
necessary to pay the direct compliance
costs incurred by the tribal
governments, or EPA consults with
those governments. If EPA complies by
consulting. Executive Order 13084
requires EPA to provide to the Office of
Management and Budget, in a separately
identified section of the preamble to the
rule, a description of the extent of EPA's
prior consultation with representatives
of affected tribal governments, a
summary of the nature of their concerns,
and a statement supporting the need to
issue the regulation. In addition.
Executive Order 13084 requires EPA to
develop an effective process permitting
elected officials and other
representatives of Indian tribal
governments "to provide meaningful
and timely input in the development of
regulatory policies on matters that
significantly or uniquely affect their
communities."
  Today's rule does not significantly or
uniquely affect the communities of
Indian tribal governments. As
mentioned above, no specific action is
required by this action. Today's rule
does not create a mandate on State, local
or tribal governments. The rule does not
impose any enforceable duties on these
entities. Accordingly, the requirements
of section 3(b) of Executive Order 13084
do not apply to this rule.

]. Congressional Review Act

  The Congressional Review Act, 5
U.S.C. 801  etseq., as added by the Small
Business Regulatory Enforcement
Fairness Act of 1996, generally provides
that before a rule may take effect, the
agency promulgating the rule  must
submit a rule report, which includes a
copy of the rule, to each House of the
Congress and to the Comptroller General
of the United States. EPA has submitted
a report containing this rule and other
required information to the U.S. Senate,
the U.S. House of Representatives, and
the Comptroller General of the United
States prior to publication of the rule  in
the Federal Register. This action is not
a "major rule" as defined by 5 U.S.C.
804(2).

List of Subjects in 40 CFR Part 261

  Environmental protection, Hazardous
materials, Waste treatment and disposal,
Recycling.
  Dated: October 30, 1998.
Carol M. Browner,
Administrator.
[FR Doc. 98-30601 Filed 11-18-98: 8:45 am]
BILLING CODE 6560-50-P

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