&EPA
                           United States
                           Environmental Protection
                           Agency
                          Office of
                          Research and Development
                          Cincinnati, OH 45268
EPA540/R-94/501a
July 1994
SITE Technology Capsule
 Filter Flow  Technology,  Inc.,
 Colloid Polishing Filter Method
Abstract

   The Filter Flow Technology, Inc. (FFT), Colloid Polish-
ing Filter Method (CPFM) was demonstrated at the U.S.
Department of Energy's (DOE) Rocky Flats Plant (RFP) as
part of the U.S. Environmental Protection Agency's (EPA)
Superfund Innovative Technology Evaluation (SITE) pro-
gram. The CPFM system Is designed to remove ionic,
colloidal, and complexed radionuclides and heavy met-
als from water. Pollutants are removed from water pre-
dominantly via sorptlon or chemical complexlng.  The
purpose of the demonstration was to evaluate the ability
of the CPFM system to remove low levels of uranium and
gross alpha contamination from RFP groundwater.

   During the demonstration, average uranium and
gross alpha  concentrations in Influent water were 98
mlcrograms per liter (^ig/L) and 91 picoCuries per liter
(pCi/L), respectively. Analytical results showed that ra-
dionuclide levels decreased by about 75% following treat-
ment with  the CPFM system. At maximum removal
efficiency, the CPFM system was capable of achieving
Colorado Water Quality Control Commission (CWQCC)
standards for water to be discharged from RFP.

   As part of the SITE program, the CPFM technology
was also evaluated based on nine criteria used for deci-
sion making in the Superfund feasibility study process.
The results of this evaluation Indicate that the CPFM
system can provide short- and long-term protection of
human health and the environment by removing radio-
nuclide contamination from water and concentrating It
in spent filter packs.
                        Introduction

                           In 1980, the U.S. Congress passed the Comprehen-
                        sive Environmental Response, Compensation, and Liabil-
                        ity Act  (CERCLA),  also  known as Superfund. CERCLA
                        committed resources to protecting human  health and
                        the environment from uncontrolled hazardous wastes
                        sites.  CERCLA was amended by the Superfund Amend-
                        ments and Reauthorization Act (SARA) in 1986 — amend-
                        ments that emphasized the achievement of long-term
                        effectiveness and permanence of remedies at Super-
                        fund  sites. SARA mandated permanent solutions and
                        alternative treatment technologies or resource recovery
                        technologies to clean up hazardous waste  sites to the
                        maximum extent possible.

                           State and federal agencies, as well as private par-
                        ties, are now exploring a growing number of Innovative
                        technologies for treating hazardous wastes. Because the
                        sites  on the National Priorities Ust comprise  a broad
                        spectrum of physical, chemical, and environmental con-
                        ditions requiring varying types of remediation, EPA has
                        focused on policy, technical, and informational issues
                        related to exploring and applying new remediation tech-
                        nologies applicable to multiple Superfund sites. One such
                        initiative is EPA's SITE program. It was established to ac-
                        celerate development, demonstration, and  use of inno-
                        vative technologies for site cleanups. EPA SITE Technology
                        Capsules summarize the latest information available on
                        selected innovative treatment and site remediation tech-
                        nologies and related issues. These capsules are designed
                        to help EPA remedial project managers, EPA on-scene
                        coordinators, contractors, and other site cleanup man-
                                   SUPERFUND INNOVATIVE
                                   TECHNOLOGY EVALUATION
                                                                            Printed on Recycled Paper

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agers understand the types of data needed to effectively
evaluate a technology's applicability for cleaning up Su-
perfund sites.

    Results from an evaluation of the CPFM system, based
on the nine criteria used for decision making in the Super-
fund feasibility study process, are presented In Table 1.
This table shows that the CPFM system provides  both
long-term and short-term protection of the environment,
reduces contaminant mobility and volume, and presents
few risks to the community or the environment.

    This Capsule provides information on the FFT CPFM
system, a technology developed to remove low levels of
radionuclldes and  heavy metal pollutants from ground-
water, wastewater, and soil washing  wastewater. The
CPFM system was evaluated under EPA's SITE program in
September  1993 at RFP in  Golden, Colorado where
groundwater Is contaminated  with radionuclldes.  Infor-
mation In this Capsule emphasizes specific site character-
istics and results of the SITE field demonstration at RFP. This
Capsule presents the following Information:

    • Technology description
    • Technology applicability
    • Technology limitations
    • Process residuals
    • Site requirements
    • Performance data
    • Technology status
    • Sources of further information

Technology Description

    The FFT CPFM system uses a proprietary compound
(Filter Flow 1000) that consists of inorganic, oxide-based
granules. Filter Flow 1000 is formulated to remove radionu-
clides and heavy metals from water through a combina-
tion of sorption, chemical complexlng, and filtration. FFT
states that sorption on the Filter Flow 1000 accounts for
the majority of the removal action.

    Filter Flow 1000 is contained In specially designed
colloid filter  packs within a colloid filter press unit. The
colloid filter press unit is approximately 7 It high and 3 ft
sq. The four filter plates of the colloid filter press unit
support three colloid filter packs. The filter plates are 26 In.
sq, 2 in. thick and constructed of very strong plastic.  One
colloid filter pack is located between each set of plates
within the colloid filter press unit. Each filter pack is  con-
structed of a durable, fibrous, polymer material that  con-
tains a premeasured amount of the complexing agent
Filter Flow  1000.  Once the filter packs have been placed
between the filter plates, hydraulic pressure is applied to
the plates. Pressure seal O-rings contained In the plates
form a water tight seal between the plates, holding water
within the unit.  The plates are  also designed to evenly
disperse water across the filter media.

   Figure 1 is a process flow diagram of the CPFM system
used for the SITE technology demonstration at RFP. The
following main components comprise the CPFM system:
an Influent mixing tank, a miniclarifier with a small sludge
filter press, a bag filter, colloid  filter press; units, and an
effluent pH adjustment tank.
    The CPFM process involves the following basic steps:
(1) contaminated water Is pumped to an Influent mixing
tank for chemical preconditioning (pH adjustment or so-
dium sulflde addition), if necessary, to Induce formation
of colloidal forms of pollutants, (2) suspended solids are
then removed by an incline plate mlnlclarifler, (3) over-
flow water from the miniclarifler Is pumped through a
mlcrofiltration bag filter where particles greater than  10
microns in diameter are removed,  (4) water passing
through the bag filter is pumped to the colloid filter press
units where heavy metals and radionuclldes are removed
by the sorption, chemical complexlng, and filtration ef-
fects of Filter Flow 1000,  (5) treated water exiting the
colloid filters is pH adjusted prior to discharge.  Following
treatment, sludge In the mlnlclarifler Is dewatered  in the
small sludge filter press using compressed  air. The filter
packs are also dewatered using compressed air to form
a cake containing 60 to 70% solids. These two solid wastes
are combined for disposal.

    During the demonstration at RFP, the  CPFM system
treated contaminated groundwater collected by an in-
tercepter  trench system constructed downgradlent  of
the RFP solar evaporation ponds. Contaminated water
from the intercepter trench Is pumped to three open-top,
500,000 gal storage tanks (the Interim measure/interim
remedial action (IM/IRA) tanks), one of which stored influ-
ent for the CPFM system. Influent pH adjustment was not
required because the influent was within the optimum pH
range (8 to 9) for the CPFM system. The pH of the effluent
water was monitored in the final pH adjustment tank and
treated with hydrochloric  acid  to  reduce the pH to  its
original level before discharge to a second IM/IRA tank.

Technology Applicability

    The CPFM technology is designed to  remove non-
tritium radionuclides and  heavy metals from water  to
parts per million  (ppm) or parts per  billion  (ppb) levels.
The CPFM  technology can be used as a stand alone unit
to treat low-total suspended solids (TSS) water or in a
treatment train, downstream from other technologies such
as soil washing, or conventional wastewater  treatment
using flocculation and solids removal. According to the
developer, potential applications also include remediation
of contaminated liquid wastes from Industrial operations,
oil-drilling production water contaminated  with naturally
occurring  radioactive materials (NORM),  uranium mine
groundwater. and transuranic and low-level radioactive
wastes from nuclear-related facilities with contaminated
water.  FFT states that the CPFM system is  designed  to
treat a  wide range of inorganic metallic  pollutants  in
water including colloidal, complexed, and ionic forms. In
general, low levels of radionuclides  and heavy metals
are the most suitable for treatment by the CPFM system.

    Under the SITE program, in addition to the full-scale
demonstration at RFP, the  CPFM system has been tested
at a bench-scale level. The study  used RFP intercepter
trench  water that contained  uranium-238 at approxi-
mately 35  pCi/L, and was spiked with up to 30 pCi/L  of
plutonlum-239, americlum-241, and radium-226. The re-
sults  from  this study indicated  removal efficiencies of
greater than 99% for uranium, plutonium, and americium
with  no chemical pretreatment. Removal  efficiency for

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Table 1.  Criteria Evaluation for the CPFM Technology
                                                                                                Criteria
Overall Protection of
Human Health and
the Envronment
Provides both short-
and long-term
protection by
efminating exposure
to contaminants in
groundwater.
Prevents off-site
migration through
sorption on filter
packs.

Compliance with
Federal ARARs
Requires compliance
with RCRA treatment,
storage, and land
disposal regulations
(of a hazardous
waste).
Wastewater discharges
require compliance
with Clean Water Act
regulations.

Long-Term
Effectiveness and
Permanence
Effectively
removes and
stabiSzes
contamination.
Involves wet-
demonstrated
technique for
removal of
contaminants.
Involves some
residuals treat-
ment (filter cake,
wastewater) or
disposal (PPE).
Reduction of
Toxhity. Mobility.
or Volume Through
Treatment
Significantly reduces
toxidty, mobiity,
and volume of
contaminants through
treatment


Short-Term
Effectiveness
Presents few
short-term risks
to workers and
community.
Some personal
protective equip-
ment required
to be worn by
operators.
The system can
relatively rapidly
reduce large vol-
umes of contam-
inated water to
dean water and
fitter cake.
Implementability Cosf
Involves few $15 per 1000
administrative gal to $0.50
difficulties. per 1000 gal
Involves few
utility require-
ments including
water, electricity,
and compressed
air.
Once on site, the
treatment system
can be oper-
ational within
1 week.
Community
Acceptance
Minimal short-term
risks presented to
the community
make this technology
favorable to the public.


State
Acceptance
If remediation is
conducted as part of
RCRA corrective
actions, state
regulatory agencies
may require permits.


   Notes:

   •Actual cost of a remediation technology is highly specific and dependent upon the original and target cleanup level, contaminant concentrations, groundwater characteristics, and volume of water. Cost dat
    presented in this table are for treating groundwater at 100 gpm for 1 year.

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                                  Mini Clarifier
                    Mixing
                    Section
             Influent
           Mixing Tank
                    -cr
                                                 Bag
                                                Filters
                                                                   Colloid
                                                                Filter Press Units
                                 F//ter Press
                               So//ds To Disposal
                      _ pH Adjustment or
                       Chemical Pretreatment
                                                 Solids
                                                   To
                                                 Disposal
                                                                                    Effluent pH
                                                                                    Adjustment Tank

                                                                                     Hydrochloric
                                          To
                                          Discharge
                        Legend
[X]

  M
           Tan/f
                            M/xer
                                               F/OJV Direction
Sample
Port
                     Note:     Colloid Filter Units can be Operated!
                              /n Series or Parallel Modes.
                              (Only Series Shown Here)
Figure 1. CPFM Treatment System.
gross alpha was 86%. These test runs showed only 43%
removal efficiency for radium.

Technology Limitations

    In general, the CPFM technology is designed to re-
move trace to moderate levels (less than 1,000 ppm) of
non-tritium radionuclides and  heavy metal  pollutants
present in water. The CPFM technology will not remove
tritium because of its chemical characteristics. Tritium in
water is incorporated in water molecules and is therefore
not retained by Filter Flow 1000. Only tritium associated
with TSS will be removed by the bag filter upstream of the
colloid filter units. Although future testing of this technol-
ogy may show differently, preliminary results and theoreti-
cal investigations do not indicate potential tritium removal.

    Because high organic compound concentrations may
interfere with the chemical and physical reactions occur-
ring between Filter Flow 1000 and charged  radionuclide
and heavy metal pollutants, water with high organic com-
pound concentrations is not treated as effectively by the
CPFM technology.

Process Residuals

    The CPFM process generates two waste streams:
treated effluent and filter cake. Demonstration analytical
results for composite samples shown  in Table 2 indicate
that effluent from runs 1  and 4 were near CWQCC dis-
charge standards for uranium and gross alpha.

    The filter cake generated  during the  demonstration
was tested for hazardous waste and radiation character-
istics and Is being stored at RFP pending  disposal at an
EPA- and DOE-approved facility. The EPA, paint filter liq-
                                                  uids test, performed at the time of waste packaging,
                                                  indicated that the wastes do not contain free liquids. The
                                                  toxicity characteristic leaching procedure was also per-
                                                  formed  on the filter cake  solids. Table 3 shows that
                                                  composited filter cake solids from the demonstration did
                                                  not contain leachable radionuclides, or leachable met-
                                                  als at levels above EPA standards (40 CFR Part 268).  In
                                                  addition. Table 4 indicates that uranium and gross alpha
                                                  activities were very low for filter cake solids  from each
                                                  run.

                                                     Drummed personal protective equipment (PPE) was
                                                  screened for radioactivity and disposed of in accordance
                                                  with state  and federal requirements. Wash water from
                                                  decontamination was collected and placed in a  1,000
                                                  gal storage tank prior to acceptance by a wastewater
                                                  disposal facility at RFP.

                                                  Site Requirements

                                                     All process equipment is mounted and operated on
                                                  the bed of a trailer. Access roads are needed for equip-
                                                  ment  transport. A paved or well graded gravel area  of
                                                  approximately 450 sq ft is also needed to accommodate
                                                  the CPFM unit, support equipment, and facilities. In addi-
                                                  tion, berms are needed for spill containment. Once on-
                                                  site, the unit can be operational within a week if all the
                                                  necessary  facilities utilities, equipment, and supplies are
                                                  available.

                                                     Utility requirements for the CPFM system are water,
                                                  electricity, compressed air, and a telephone. Clean pro-
                                                  cess water Is required for system operation and decon-
                                                  tamination of equipment and personnel. Fire hydrant
                                                  water was provided by the site operator for the demon-
                                                  stration. The CPFM system used for the demonstration

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Table 2. Analytical Results from the CPFM SITE Demonstration
                               Influent
                       Intermediate
Effluent
Parameter Run
Number
Uranium (ng/L) 1
Gross Alpha (pCi/L)
Uranium (pg/L) 2
Gross Alpha (pCi/L)
Uranium (ng/L) 3
Gross Alpha (pCi/L)
Uranium fyig/L) 4
Gross Alpha (pCi/L)
Composite/
Duplicate
102/104
98/99
89/94
88/62
102
110
98
65
Grab/
Duplicate
102
94
102
110
96/96
100/110
104
100
Composite/
Duplicate
60/60
40
92
84
94
36
64
71
Grab/
Duplicate
62
77
98/94
68/110
94/92
110/57
55
50
Composite/
Duplicate
9.5/9.6
13
38/38
53/47
23/25
27
5.1
3.7
Grab/
Duplicate
3.4
9.4
43
24
7.9/8.3
0/25
19
11
CWQCC*
Standards
7
7
7
7
7
7
7
7
* Colorado Water Quality Control Commmission
 Table 3. Analytical Results for TCLP Extract Solutions
    Parameter
Run 5 Pack 1
                                                        Run 5 Pack 2
                                                 Regulatory Level (mg/L)
Uranium (fig/L)
Gross Alpha (pCi/L)
Arsenic (iig/L)
Barium (pg/L)
Cadmium (ng/L)
Chromium (ng/L)
Lead(fig/L)
Mercury (pg/L)
Selenium (ng/L)
Silver (\ig/L)
1.0U
82U
380U
2,640
SOU
40U
290U
10U
10U
40U
1.0U
290U
380U
4,780
SOU
40U
290U
10U
10U
40U
	
—
6.0
100.0
1.0
5.0
5.0
0.2
1.0
5.0
U = undetected at this value
Table 4. Analytical Result for Filter Pack Solids
Parameter
Uranium (pg/g)
Gross Alpha (pd/g)
Run 1
2.1
13U
Run 2
2.1
12
Run 3
3.4
15
Run 4
Packl
2.6
8.1
RunS
Pack 2
4.7
11
RunS
5.7
12U
U = undetected at this value
requires 120-volt,  30-amperes electrical service  and a
minimum of 100 psi compressed air supply for the process
equipment and field laboratory equipment. For the dem-
onstration, gas powered generators and an air compres-
sor were used. Telephone service is  required mainly for
ordering equipment, scheduling deliveries, and commu-
nicating emergencies.  A cellular telephone  was used
during the demonstration,

   Additional equipment and supplies included a 1,000-
gal water storage tank  for decontamination rinse water.
equipment for filter cake disposal. Including 66-gal drums
and  a forklift with operator, sampling equipment and
containers, and health-  and safety-related  gear.
                            After treatment Is completed, the treatment system
                        can be demobilized within 1 week. This activity includes
                        equipment decontamination and utilities disconnection.
                        Demobilization following the demonstration took approxi-
                        mately 1 week.

                        Performance Data

                            The CPFM technology was developed to treat water
                        contaminated with radionuclides and heavy metals. Wa-
                        ter from the RFP IM/IRA storage  tanks was selected  as a
                        source of contaminated water for the demonstration be-
                        cause the principal  contaminants in groundwater at RFP
                        were expected to be uranium, radium, plutonium, and

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americium. Following the bench scale testing, the con-
tamination in RFP water was determined to be  domi-
nantly uranium and gross  alpha. Therefore,  these
contaminants were  considered the critical parameters
and radium, plutonlum, and americium were considered
secondary parameters.

    The CPFM technology was evaluated to determine
appropriateness for  use in removing radlonuclides from
RFP water. The objectives for the project were to:

    •  Assess the technology's ability to remove uranium
      and gross alpha contaminants to levels below
      CWQCC standards
    •  Document the operating conditions, and identify
      operational needs, such as utility and labor re
      quirements, for the treatment system
    •  Estimate costs associated with the operation of
      the CPFM system
    •  Assess the technology's ability to remove other
      radlonuclides (plutonlum, americium, and radium)
    •  Evaluate the disposal options for preflltered solids
      (miniclarlfler and bag filter solids) and spent filter
      packs from the colloid filter unit

    The demonstration was comprised of three tests. The
first test consisted of three replicate runs of 4 hr each, at
operating parameters established  by the developer.
Three  runs were conducted during this test in order to
collect enough  data to statistically evaluate the  CPFM
system's ability  to meet CWQCC standards. For these
runs, the colloid filter presses held three filter packs each
and water was  routed through the packs In series. Dur-
ing these three  runs, process parameters Including flow
rate (5 gal/mln), and amount of filter bed material  (30
kilograms of Filter Flow 1000) were held constant. For the
second test, sodium sulfide was added to the influent
water in the pretreatment tank to change the oxidation
state of radlonuclides in water. This test consisted of one
run; using the same operating configuration and condi-
tions as the first test. The purpose  of this test was to
determine whether pretreatment could be used  to im-
prove CPFM performance that may be required  to at-
tain CWQCC standards. The third test was a 15-hr run.
This test used only  a single pack in each colloid filter
press.  This run was  designed to  determine the time of
breakthrough and the amount of contamination each
filter pack is capable of treating. This information was
then used  in evaluating the operational costs of  the
CPFM system.

    During the demonstration, samples were collected
of the untreated water (influent), pretreated water after
passing through the miniclarifier and bag filter (interme-
diate), and treated water that had passed through  the
filter packs (effluent). Filter cake  was also  analyzed.
Samples were analyzed to determine the technology's
effectiveness and evaluate disposal options for filter cake.

    Analytical results for uranium and gross alpha from
runs 1  through 4 are presented in Table 2. Runs 1  through
4 were designed to collect sufficient data to do a statis-
tical evaluation of CPFM system capabiliHes. Therefore,
composite, grab, and replicate samples v/ere collected
and analyzed.

    Assessment  of data quality for the critical param-
eters uranium and  gross alpha included evaluation of
laboratory method blanks, matrix spike and matrix spike
duplicate recoveries, and analytical/field duplicates. No
laboratory contamination was Indicated by method blank
data. Uranium matrix spike recoveries were all within the
acceptable range of 80 to  120%. However, 3 out of 20
matrix spike recoveries for gross alpha were outside of
these control  limits. Duplicate uranium analyses were all
well  within ±  20%. Samples  and duplicates  yield an r2
value from linear regression  of 0.99, Indicating that ura-
nium analyses had good precision. However, 12 out of 20
duplicate gross alpha analyses exceeded + 20%. Samples
and duplicates yield an r2 value from linear regression of
0.15, Indicating poor precision of gross alpha data. There-
fore, only uranium analyses are considered  reliable for
assessing the performance of the CPFM system and gross
alpha data should be Interpreted with caution.

   Figures 2 and  3 show graphically the removal of ra-
dionuclides in runs 1 through  4. Figures 4 and 5 show gross
alpha and uranium concentrations, respectively, for sam-
pling during the breakthrough assessment of run 5. Where
possible, only composite  data were used to construct
these figures (where replicate composites exist, an aver-
age  value was used). Composite gross alpha and ura-
nium concentrations for influent for runs 1 through 3, varied
from 62 to 110 pCI/L for gross alpha and 89 to 104 ng/L for
uranium. Analytical results for composite samples of Inter-
mediate waters from these three runs show a range of 36
to 84 pCI/L for gross alpha and a range of 60 to 94 ja.g/L
for uranium. Analytical results for composite effluent wa-
ter from runs  1 through 3 show gross alpha values that
range from a low of 13 pCi/L for run 1 to a high of 53 pCi/
L for  run 2. Similarly, analytical results for uranium ranged
from a low of 9.5 ng/L for run 1 to a high of 38 jig/L for run
2.

   Removal efficiencies for runs 1 through 4 were calcu-
lated using composite data and are shown in Table 5.
(Where replicate composites exist, an average value was
used.) Overall removal efficiencies for uranium during runs
1 through  3  ranged from a low of 58.4% to a  high of
90.6%. Overall removal efficiencies for gross alpha for runs
1 through 3 ranged between 33.3% and 86.8%.  Overall
removal efficiencies for uranium and gross alpha for run 4
were slightly better than the best of the initial 3 runs (run
1) with 94.8%  and 94.3%  removal, respectively. It should
be noted that only in run 4 were the CWQCC standards
for composite sampling met. Though removal Is largely
attributable to the colloid filter pack, significant removal
of uranium occurred in runs 1 and 4 prior to the colloid
filter  unit. Significant pre-colloid filter removal of gross
alpha is also indicated for runs 1 and 3.

   Analytical results for plutonium and americium showed
that  these elements were at or near method detection
limits. Therefore, the ability of the CPFM system to remove
them from RFP groundwater could not be properly evalu-
ated. Results for radium analyses indicated that the CPFM
system did not remove radium from RFP groundwater.

   The results from run 5, the breakthrough run, are pre-
sented graphically in Figures 4 and 5. These result Indicate
that  using a  single colloid filter  unit, breakthrough oc-
curred prior to the first sampling time at 120 min  or that
the single pack was not capable of removing significant
contamination. This result was not expected  based on
the information Initially provided by FFT. On average, only
a slight reduction in the influent uranium and gross alpha

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          I

          I

          1
                 120
                 100  .
                  80  .
  60  .
 40  _
                  20
                                                                             Run 1
                                                                             Run 2
                                                                             Run 3
                                                                        E3   Run 4
                                Influent
                                           Intermediate
                                                                                          Effluent
Figure 2. Gross alpha concentrations for runs 1 through 4.
           c"
           ;§

           £

           §

           §

           I


           I
               120
               100
                80
60
40
20
                                 Influent
                                           Intermediate
                                                                                           Effluent
Figure 3.  Uranium concentrations for runs 1 through 4.

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Gross Alpha
Concentration
(pCi/L) Removal
Efficiency
1 o/ \
160 _
140 .
120 .
100 ,
80
60 .
40 .
20 .
0
( '°
Mean Influent
Mean Intermediate (12)
//
/



Mean ~~
Effluent
120 240 360 480 540 600 660 720 780 840 900
1


0
- 40
- 60
- 80
100
Time (minutes)
Figure 4.  Gross alpha concentrations for run 5 effluent. Solid squares correspond to concentrations and removal efficiencies.
Uranium
Concentration Removal
(mg/L) Efficiency
(%)
140 -
120 ,
100 _
80 .
60

40 .
20 -
0
r Mean Influent Mean Intermediate (L2)

•._-— -••~"— "'"•"—•-— --.p.-— — -B"" »~><-*»^ •_^-**^
•^ ' / .
Mean Effluent

m

I I I 1 I I I I I I

0
- 20
- 40

- 60
- 80
100
120 240 360 480 540 600 660 720 780 840 900
                                                  Time (minutes)
Figure 5.  Uranium concentrations for run 5 effluent. Solid squares correspond to concentrations and removal efficiencies.

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Table 5. Removal Efficiency Results for Runs 1 through 4 for the CPFM SITE Demonstration
Parameter
Uranium (ng/L)
Gross Alpha (pCi/L)
Uranium (ng/L)
Gross Alpha (pCi/L)
Uranium (fig/L)
Gross Alpha (pCi/L)
Uranium (ng/L)
Gross Alpha (pCi/L)
* Overall removal et
Run
Number
1
2
3
4
ficiency —

Influent
103
98.5
91.5
75
102
110
98
65
Intermediate
60
40
92
84
94
36
64
71
Effluent
9.6
13
38
50
24
27
5.1
3.7
CWQCC
Standards
7
7
7
7
7
7
7
7
Mini-Clarifier
and Bag
niter
Removal
Efficiency
41.7
59.4
-0.5
-12.0
7.8
72.5
34.7
-9.2
Colloid
Filter Unit
Removal
Efficiency
84.0
67.5
58.6
40.5
74.5
25.0
92
94.8
Overall
Removal
Efficiency
90.6
86.8
58.4
33.3
76.5
75.5
94.8
94.3
[Influent! - \Effluentf x WQ
[Influent]
 ' Colloid Filter Unit
  removal efficiency =
flntermediate] - [Effluent]
    [Intermediate]
x 100
Where: [] equals the concentration of the individual parameters
concentrations was observed In run 5. It should be noted
that data for this run  are erratic, thus indicating  that
performance of the system during discrete time intervals
may be unpredictable. Single pack removal efficiencies
are considerably less than the series of six packs used in
runs 1 through 4.  Reduction in removal efficiencies may
be due to a variety of factors such as channeling through
a  single pack, or Insufficient residence time within the
pack. However, this demonstration was not designed  to
evaluate such factors.

    Operating conditions documented during the dem-
onstration indicated that water treatment with a series of
colloid filter packs was successful  In  removing uranium
and gross alpha contamination from RFP waters. The dem-
onstration results also indicate that pretreatment of influ-
ent water  with sodium sulfide improves CPFM system
removal efficiencies.

    Disposal options  for the used filter pack are deter-
mined by Its radionuclide and leachable metal content.
Table 4 shows that concentrations of uranium in the filter
cake ranged from 2.1 to  5.7 ng/g and gross alpha con-
centrations ranged from not detectable to 15 picoCuries
per gram  (pCi/g). In addition. Table  3 shows TCLP test
results Indicating that the filter cake does not contain
extractable metals above regulatory limits.

    Based on an economic analysis using a 1 -year treat-
ment scenario at 100 gal/min for 24 hr/day,  7 days/wk,
the treatment cost is approximately  $15/1000 gal. This
cost Is reduced to $0.50/1000 gal using a  5-yr treatment
scenario. Costs can be expected to vary depending on
contamination type, level, and volume of water treated.

Technology Status

    Ottier sites are considering the CPFM system. Pilot-
scale testing Is underway at the Oak Ridge National Labo-
ratory through a joint venture with Martin Marietta  and
Dwight and Church. The pilot test will determine the CPFM
process effectiveness in treating mixed waste. In another
                                 pilot-scale test, funded by the Westlnghouse Science and
                                 Technology Group, the process Is being applied in a treat-
                                 ment train to mixed wastewater that has been pretreated
                                 to destroy organic compounds and remove suspended
                                 solids. The CPFM system is also being used to treat metal
                                 finishing wastes. FFT is also building a CPFM system in Peru
                                 that will treat mine wastewater discharge that contains
                                 copper, zinc, lead, and arsenic. In all, a total of 15 com-
                                 mercial projects are planned or underway.

                                 Sources of Further Information

                                 EPA Contact:

                                        U.S. EPA Project Manager:
                                        Annette Gatchett
                                        U.S. Environmental Protection Agency
                                        Risk Reduction Engineering Laboratory
                                        26 West Martin Luther King Drive
                                        Cincinnati, OH 45268
                                        Telephone No.: 513/569-7697
                                        Fax No.: 513/569-7620

                                 Technology Developer:

                                        Tod Johnson, Ph.D.
                                        Filter Flow Technology, Inc.
                                         122 Texas Avenue
                                        League City, TX 77573
                                        Telephone No.: 713/554-5405
                                        Fax No.: 713/554-5208

                                 DOE Contact:

                                        Beth Brainard-Jordan
                                        Community Relations
                                        DOE Rocky Flats Office
                                        Rocky Flats Plant
                                        P.O. Box 928
                                        Golden, CO 80402-0928
                                        Telephone No.: 303/966-5993

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United States
Environmental Protection Agency
Center for Environmental Research Information
Cincinnati, OH 45268

Official Business
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$300
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