vvEPA
             United States
             Environmental Protection
             Agency
            Hazardous Waste Engineering
            Research Laboratory
            Cincinnati OH 45268
EPA/600/2-86/001
January 1986
             Research and Development
Underground Tank
Leak Detection
Methods:

A State-of-the-Art
Review

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                                        EPA/600/2-86/001
                                        January 1986
    UNDERGROUND TANK LEAK DETECTION METHODS:
           A STATE-OF-THE-ART REVIEW
                       by
      Shahzad Niaki and John A. Broscious
                 IT Corporation
        Pittsburgh, Pennsylvania  15235
            Contract No. 68-03-3069
                Project Officer
                 John  S.  Farlow
            Releases Control Branch
Hazardous Waste Engineering Research Laboratory
           Edison, New Jersey  08837
HAZARDOUS WASTE ENGINEERING RESEARCH LABORATORY
      OFFICE OF RESEARCH  AND  DEVELOPMENT
      U.S.  ENVIRONMENTAL PROTECTION  AGENCY
             CINCINNATI,  OH  45268
                                                     Protection *••"<*
                                   230  South Dearborn Street
                                   Chicago, Illinois  60604

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                                       DISCLAIMER
             The information in this  document has been funded wholly or in part
        by the United States Environmental  Protection Agency under Contract No.
        68-03-3069 to IT Corporation.   It has been subject to the Agency's peer
        and administrative review,  and it has been approved for publication as
        an EPA document.  Mention of  trade  names or commercial products does not
        constitute an endorsement or  recommendation for use.
U,S. Environmental Protection Agency

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                                FOREWORD
     Today's rapidly developing and changing technologies and industrial
products and practices frequently carry with them the increased gener-
ation of solid and hazardous wastes.  These materials, if improperly
dealt with,  can threaten both public health and the environment.
Abandoned waste sites and accidental releases of toxic and hazardous
substances to the environment also have important environmental and
public health implications.  The Hazardous Waste Engineering Research
Laboratory assists in providing an authoritative and defensible engi-
neering basis for assessing and solving these problems.  Its products
support the policies, programs, and regulations of the Environmental
Protection Agency, the permitting and other responsibilities of State
and local governments, and the needs of both large and small businesses
in handling their wastes responsibly and economically.

     This report describes both commercially available and developing
techniques for detecting leaks in underground storage tanks, and will be
useful to government officials, industry, and those members of the
public concerned with this aspect of preventing the pollution of ground
water.

     For further information, please contact the Land Pollution Control
Division of the Hazardous Waste Engineering Research Laboratory.
                                  David G. Stephan, Director
                        Hazardous Waste Engineering Research Laboratory
                                   ill

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                                PREFACE
     This report  has been prepared by IT Corporation (IT) under contract
with the U.S.  Environmental Protection Agency (EPA), to be used as a
state-of-the-art  overview of available and developing leak detection
methods for testing underground tank, systems.  The descriptions of
detection methods and the techniques to compensate for the effects of
the variables  affecting detection methods have been reviewed by the man-
ufacturer, practitioner, or developer of the detection method.  It is
expected that  this report will result in further evaluation in detection
methods to compensate for variables affecting the accuracy of available
and developing detection methods.

     The variables described in this report should be considered as
potential sources of error, especially in the application of volumetric
leak detection methods.  The applicability and effectiveness of
detection methods identified must be determined on an individual test
situation basis.   The applicability of a detection method will depend
upon numerous  factors including hydrogeologic, economic, climatic, and
conditional considerations.

     As an aid to identifying all of the available and developing leak
detection methods for underground tank testing, a list of the identified
detection methods was published by the Petroleum Equipment Institute
(PEI) in its Tulsa letter in August 1984 (together with the request that
IT be advised  of  any other detection methods).  In addition, a limited
patent search  was conducted to identify other leak detection methods for
testing underground tanks or tank systems.
                                   iv

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                                ABSTRACT
     This report is a state-of-the-art review of available and develop-
ing methods for finding small leaks in underground storage tanks used
primarily for gasoline and other liquid petroleum fuels.  This review
describes (based on information provided by the manufacturers or practi-
tioners) a total of thirty-six volumetric, nonvolumetric, inventory mon-
itoring, and leak effects monitoring detection methods; provides general
engineering comments on each volumetric and nonvolumetric leak detection
method; and discusses variables which may affect the accuracy of
detection methods.  The emphasis throughout is on volumetric and
nonvolumetric leak detection methods.

     This report was submitted in fulfillment of Contract No. 68-03-3069
by IT Corporation under the sponsorship of the U.S. Environmental Pro-
tection Agency.  This report covers a period from July 1984 to January
1985, and work was completed as of June 1985.

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                                CONTENTS
                                                                  PAGE
DISCLAIMER                                                          ii
FOREWORD                                                           iii
PREFACE                                                             iv
ABSTRACT                                                             v
FIGURES                                                             xi
TABLES                                                             xii
ACKNOWLEDGEMENT                                                   xiii

     SECTION 1 - INTRODUCTION                                        1
                   STATEMENT OF THE PROBLEM                          1
                   REPORT OBJECTIVE                                  2
     SECTION 2 - SUMMARY                                             3
     SECTION 3 - CONCLUSIONS                                        26
     SECTION 4 - RECOMMENDATIONS                                    27
     SECTION 5 - VARIABLES AFFECTING LEAK DETECTION METHODS         28
                   VOLUMETRIC LEAK DETECTION TESTS                  28
                     Temperature                                    35
                     Water Table                                    35
                     Tank Deformation                               37
                     Vapor Pockets                                  42
                     Product Evaporation                            42
                     Piping Leaks                                   42
                     Tank Geometry                                  42
                     Wind                                           44
                     Vibration                                      44
                     Noise                                          44
                                   vii

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                Equipment Accuracy                             45
                Operator Error                                 45
                Type of Product                                45
                Power Variation                                45
                Instrumentation Limitation                     45
                Atmospheric Pressure                           46
                Tank Inclination                               46
              NONVOLUMETRIC LEAK TESTS                         46
                Temperature                                    46
                Water Table                                    47
                Tank Deformation                               47
                Vapor Pocket                                   48
                Product Evaporation                            48
                Piping Leaks                                   48
                Tank Geometry                                  48
                Wind                                           48
                Vibration                                      48
                Noise                                          48
                Equipment Accuracy                             49
                Operator Error                                 49
                Type of Product                                49
                Power Variation                                49
                Instrumentation Limitation                     49
                Atmospheric Pressure                           49
                Tank Inclination                               49
                General Problems                               49
              INVENTORY CONTROL                                50
              LEAK EFFECTS MONITORING                          50
SECTION 6 - LEAK DETECTION METHODS REVIEW                      51
              CLASSIFICATION                                   51
                Volumetric (Quantitative) Leak Testing         52
                Nonvolumetric (Qualitative) Leak Testing       52
                             viii

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  Inventory Control                              52
  Leak Effects Monitoring                        52
LEAK DETECTION TESTING METHODS                   52
  Volumetric (Quantitative) Leak Testing         52
  Methods
   1- Ainlay Tank Tegrity Testing (TTT)          52
   2- ARCO HTC Underground Tank Leak Detector    56
   3- Certi-Tec Testing                          60
   4- "Ethyl" Tank Sentry Testing                63
   5- EZY-CHEK Leak Detector                     66
   6- Fluid-Static (Standpipe) Testing           71
   7- Heath Petro Tite Tank and Line Testing     72
      (Kent-Moore Testing)
   8- Helium Differential Pressure Testing       76
   9- Leak Lokator LD-2000 Test (Hunter-         77
      Formerly Sunmark Leak Detection)
  10- Mooney Tank Test Detector                  82
  11- PACE Leak Tester                           84
  12- PALD-2 Leak Detector                       87
  13- Pneumatic Testing                          89
  14- Tank Auditor                               90
  15- Two-Tube Laser Interferometer System       93
  Nonvolumetric (Qualitative) Leak Testing       96
  Methods
   1- Acoustical Monitoring System (AMS)         96
   2- Leybold-Heraeus Helium Detector,           97
      Ultratest M2
   3- Smith & Denison Helium Test                98
   4- TRC Rapid Leak Detector for Underground    100
      Tanks and Pipes
   5- Ultrasonic Leak Detector, Ultrasound       100
   6- VacuTect (Tanknology)                      102
   7- Varian Leak Detector (SP Y2000 or 938-41)  103
   Inventory Monitoring                          105
   1- Gage Stick                                 105
                ix

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                      2- MFP-414  TLG  Leak Detector                  105
                      3- TLS-150  Tank Level  Sensor  (Veeder-Root)   108
                     Leak  Effects Monitoring                       109
                      1- Collection  Sumps                          109
                      2- Dye  Method                                 109
                      3- Ground Water or Soil  Core  Sampling        111
                      4- Interstitial Monitoring in Double-        111
                        Walled Tanks
                      5- LASP Monitoring System (Leakage Alarm     112
                        System for  Pipe)
                      6- Observation Wells                         112
                      7- Pollulert and Leak-X Detection Systems    114
                      8- Remote Infrared Sensing                   114
                      9- Surface  Geophysical Methods               114
                     10- U-Tubes                                    114
                     11- Vapor Wells                               116
REFERENCES                                                         118
APPENDIX - LEAK DETECTION  METHODS - MANUFACTURER OR PRACTITIONER
           PHONE NUMBERS
                                    x

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                                FIGURES

FIGURE NO.                            TITLE                        PAGE
    1        Temperature Stratification                             29
    2        Average Gasoline Temperature for All Test Stations     30
    3        Mean Temperature Distribution as a Function of Depth   31
             for Four Different 24-Hour Periods
    4        Tank Temperature Stratification and Gradients for a    32
             24-Hour Period After  Tank Fill Up
    5        Location of Temperature Sensors in the SRI Tank        33
    6        Delivery Temperatures                                  34
    7        Tank End Deflection                                    38
    8        Change in Tank Volume Due to Tank End                  39
             Deflections - In Gallons
    9        Examples of Three Common Vapor Pockets                 43
    10       Ainlay Tank Tegrity Testing Method                     53
    11       ARCO Underground Tank Leak Detector                    57
    12       Certi-Tec Tank Testing System                          61
    13       "Ethyl" Tank Sentry Kit                                64
    14       "Ethyl" Tank Sentry Installation                       64
    15       EZY-CHEK Leak Detector                                 67
    16       EZY-CHEK Leak Detector Installation                    68
    17       EZY-CHEK Leak Detector Temperature Averaging Probe     68
    18       Petro Tite Installation                                73
    19       Leak Lokator Installation                              78
    20       Two-Tube Laser Interferometer                          94
    21       MFP-414 TLG Leak Detector-Sensor Assembly             106
    22       MFP-414 TLG Tank Level Gauge & Leak Detector          107
    23       Typical Wells for Continuous Gas or Vapor Monitoring  110
    24       Examples of Observation Wells                         113
    25       Example of a U-Tube Installation                      115
                                   xi

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                                 TABLES
TABLE NO.                           TITLE                          PAGE

    1       Volumetric Leak Detection Methods - General               5
            Information

    2       Nonvolumetric Leak Detection Methods - General            8
            Information

    3       Other Leak Detection Methods - General Information       10

    4       Volumetric Leak Detection Methods - General
            Capabilities                                             12

    5       Nonvolumetric Leak Detection Methods - General           14
            Capabilities

    6       Other Leak Detection Methods - General Capabilities      15

    7       Volumetric Leak Detection Methods - Compensation         16
            for Effects of Variables

    8       Nonvolumetric Leak Detection Methods - Compensation      22
            for Effects of Variables

    9       Other Leak Detection Methods - Compensation for          24
            Effects of Variables

    10      Thermal Expansion of Liquids                             36

    11      Pressure-Height Chart                                    40
    12      Total Force on Tank Ends                                 40

    13      Apparent Loss of Product Volume Due to Force on Tank     41
            Ends - In Gallons
                                 xii

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                            ACKNOWLEDGEMENT
     This report was prepared by IT Corporation, Pittsburgh,
Pennsylvania.  The authors wish to express their indebtedness to Mr.
John S. Farlow, the U.S. Environmental Protection Agency's (EPA) Project
Officer, for his constant cooperation which assisted in the preparation
of this report.

     The authors wish to acknowledge the valuable contribution of many
people and organizations, including the American Petroleum Institute
(API), the Petroleum Equipment Institute (PEI), and the underground tank
leak detection manufacturers or developers which were contacted.  In
particular, the authors would like to thank those individuals on the
Environmental Protection Agency Technical Review Committee, including
Mr. James H. Pirn, Suffolk County Department of Health Services; Mr.
Andres Talts, Department of Defense; Mr. William E. Blain and Mrs. Diane
English, New York Department of Environmental Conservation; Mr. Steven
Way, EPA Office of Solid Waste; and Mr. David Chin, EPA Region I, who
provided valuable comments and suggestions on the report outline and
text.
                                  xiii

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                               SECTION  1

                              INTRODUCTION
STATEMENT OF THE PROBLEM

     In recent years, the increase in leaks from underground gasoline
storage tanks has had a significant adverse environmental impact on the
United States.  Current estimates from government and industry sources
are that between 1.5 to 3.5 million underground storage tanks exist in
the nation.  Estimates of the number of leaking tanks range from 75,000
to 100,000; and 350,000 others may develop leaks within the next five
years (1).  The 1983 National Petroleum News Factbook Issue forecasts
the existence of approximately 140,000 gasoline service stations in the
United States at the end of 1983.  New York State estimates that 19
percent of its 83,000 active underground gasoline tanks are now leak-
ing.  Maine estimates that 25 percent of its 1,600 retail gasoline
underground tanks are leaking approximately 11 million gallons yearly.
In Michigan 39 percent of ground water contamination incidents are
attributed to storage tanks.

     One of the primary causes of tank leakage is corrosion of the stor-
age tanks.  Product loss from leaking tanks may cause an adverse effect
on the environment, endanger lives, reduce income, and require the ex-
penditure of millions of dollars for cleanup.  To prevent or reduce the
adverse effects of gasoline leakage, an accurate method must be used to
determine whether or not an underground tank is leaking.

     The 1984 Resource Conservation and Recovery Act (RCRA) amendments
regulate underground storage tanks containing petroleum products and
substances defined in Comprehensive Environmental Response,
Compensation, and Liability Act (CERCLA).  RCRA regulations specify
release detection, prevention, and corrections and require a leak
detection system, an inventory control system, and a tank testing (or
equivalent system).  States are also passing legislation and writing
regulations requiring both staged replacement of existing underground
tanks and installation of monitoring wells to detect leaks.  Performance
standards for new tanks will be specified under RCRA and included in
various state regulations.

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REPORT OBJECTIVE

     The objective of this report is to identify existing and developing
techniques to detect leaks in underground fuel storage tanks.  This
objective is accomplished by a review of the manufacturer's description
of each method, its capabilities, and its claimed precision and
accuracy.

     The variables affecting leak detection methods are introduced in
Section 5.  This information should give the reader an understanding of
the major variables and their effects on the accuracy of various leak
detection methods.  Section 6 presents a description of each detection
method based on the available literature from the manufacturer (or
practitioner).  The descriptions in Section 6 of the manufacturer's
techniques for offsetting the effects on each detection method of these
major variables are based on information from the manufacturer's liter-
ature, reports, and/or verbal communications between the authors and the
staff of the manufacturer.  This information was reviewed for correct-
ness by most of the manufacturers, practitioners, or developers of the
detection methods (instruments).  Independent engineering evaluations of
error sources for each detection method are provided by the authors.
Finally, Tables 1 through 9 in Section 2 summarize the capabilities of
the leak detection methods.  Information in these tables is primarily
from each manufacturer's description and, where noted, from the engi-
neering comments in Section 6.  The appendix at the end of this report
provides the phone number and contact name of the manufacturer/
practitioner for each manufactured leak detection method.

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                               SECTION 2

                                SUMMARY
     Existing and developing leak detection methods were reviewed, and
techniques for offsetting the effects of variables which affect accuracy
were evaluated.  In Tables 1 through 9, general information, general
operational capabilities, and compensation for effects of variables dis-
cussed in this text are summarized for volumetric, nonvolumetric, and
other leak detection methods for underground storage tanks.  Wherever it
is appropriate, in these summary tables, the information furnished is
based on engineering comments and not the manufacturer's claim.

     To conduct this survey, the American Petroleum Institute (API) and
the Petroleum Equipment Institute (PEI) were contacted for assistance in
developing a comprehensive list of available detection methods.  A
limited patent search was performed to identify methods currently being
developed, but not yet available commercially.  In all, fifteen volu-
metric leak testing, seven nonvolumetric leak testing, three inventory
monitoring, and eleven leak effects monitoring methods were found.

     The information on the following pages (Tables 1 through 9) is
based almost entirely on information provided by the manufacturers and
practitioners of the detection methods.

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                                     TABLE 1.  VOLUMETRIC LEAK DETECTION METHODS - GENERAL  INFORMATION
Method
          Description
1.  Ainlay Tank Tegrity
    Testing
2.  ARCO HTC Underground
    Tank Leak Detector
3.  Certi-Tec Testing
4.  "Ethyl" Tank Sentry
5.  EZY-CHEK Leak Detector
6.  Fluid-Static (Stand-
    pipe) Testing
                                   Principle
• Pressure measurement by
  a coil type manometer,
  determine product level
  change in a propane
  bubbling system

• Level change measurement
  by float and light sensing
  system

• Monitors pressure changes
  resulting from product
  level changes

• Level change magnification
  by a "J" tube manometer
  Pressure measurement,
  determine product level
  change in an air bubbling
  system

  Pressurize a system by
  a standpipe
  Keep the level constant
  by product addition or
  removal
  Measure rate of volume
  change
                               Claimed Accuracy  Calibration
                                   (gal/hr)      During Test
                                                                   0.02
                                                                   0.05
                                                                   0.05
 Sensitive to
 0.02  inches
 level change

Less than 0.01
     Gross
                                                                                   Yes
                                                                                   Yes
                                                                                    No
                                                                                    No
                                                                                   Yes
                      No
                                     Cost  of
                                     Testing*

                                  $225/day  + Exp.
                                  3  tanks/day  (8)
$300/tank (17)
                                                                  $300/tank (19)
                                                                                                      Low
                      Single Tank
                      Preparation
                        for Test

                  Fill a tank evening
                  before a test
                                                    Adjust the level at
                                                    66-76 percent
                                                                                                                  None
No deliveries 24
hours prior to a
test

Fill up four hours
prior to a test,
usually test at
night

Fill the tank prior
to a test
                                                                                                                            (continued)

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                                                           TABLE  1  (continued)
Method
          Description
                                   Principle
                                                        Claimed Accuracy   Calibration         Cost  of
                                                            (gal/hr)       During Test        Testing*
                                                                                        Single Tank
                                                                                        Preparation
                                                                                          for Test
 7.
Heath Petro Tite Tank
and Line Testing (Kent-
Moore)
 8.
 9.
Helium Differential
Pressure Testing
     Leak Lokator Test
     Hunter-Formerly
     Sunmark Leak
     Detection
• Pressurize a system by a
  standpipe
• Keep the level  constant
  by product addition or
  removal
• Measure volume  change
• Product circulation by
  pump

• Leak detection  by  differ-
  ential pressure change in
  an empty tank
• Leak rate estimation by
  Bernoulli's equation

• "Principle of Buoyancy"
  The apparent loss  in
  weight of any object
  submerged in a  liquid
  is equal to the weight
  of the displaced volume
  of liquid
                                                              Less than 0.05
                                                                                   Yes
                                $75/1,000 gal  (21)
Less than 0.05
                                                          0.05 even at
                                                            product
                                                            level at
                                                           the center
                                                           of a  tank
                                                                                    No
                                                                                   Yes
                                  $500/tank (25)
                                                                                                                  Fill the tank prior
                                                                                                                  to a test
                                                                                                                  Seal the ports to
                                                                                                                  the atmosphere,
                                                                                                                  empty the tank
Typically fill the
tank before testing
(if it is possible
to fill a tank by
the product)
10.   Mooney Tank Test
     •Detector
11.  PACE Tank Tester
                         • Level change measurement           0.02
                           with a dip stick
                         • Magnification of pressure       Less than
                           change in a sealed  tank            0.05
                           by using a tube and based
                           on manometer principle
                                                     Yes
                                                                                   Yes
                                  $250/tank (27)
                                                                                                Not Commercial
                                                                                    Fill the tank 12-14
                                                                                    hours prior to a
                                                                                    test

                                                                                    • Fill the tank 12
                                                                                      hours prior to a
                                                                                      test
                                                                                    • Seal all the ports
                                                                                      except fill pipe
                                                                                                                            (continued)

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                                                          TABLE 1 (continued)
Method
          Description
                                   Principle
                               Claimed Accuracy  Calibration          Cost  of
                                   (gal/hr)      During Test         Testing*
                                                        Single Tank
                                                        Preparation
                                                          for Test
12.  PALD-2 Leak Detector
13.  Pneumatic Testing
14.  Tank Auditor
15.  Two-Tube Laser Inter-
     ferometer System
• Pressurize system with
  nitrogen at three dif-
  ferent pressures
• Level measurement by
  an electro-optical
  device
• Estimate leak rate
  based on the size of
  leak and pressure
  difference across the
  leak

• Pressurize system with
  air or other gas
• Leak rate measurement
  by change in pressure

• "Principle of Buoyancy"
                                                              Less than 0.05
                                                                                    No
                                  Not commercial
  Level change measurement
  by laser beam and its
  reflection
    Gross
0.00001 in the
   fill  pipe
  0.03  at  the
  center of a
  10.5-foot-
 diameter  tank

Less than 0.05
                      No
                                                                                    Yes
                                        Low
                      Yes
                  Fill the tank 24
                  hours prior to a
                  test.  All ports
                  must be hermetic-
                  ally sealed
                                                    Seal the ports
  $400/tank       None
Not Commercial    None
^Charges could be negotiated with manufacturer for different numbers of tank testing and different tank  specifications.
(  )See References.

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                                       TABLE  2.  NONVOLUMETRIC LEAK DETECTION METHODS  - GENERAL  INFORMATION
      Method
                Description
oo
      1.  Acoustical Monitoring
          System (AMS)
      2.
Leybold-Heraeus Helium
Detector, Ultratest M2
      3.
Smith & Denison Helium
Test
      4.
TRC Rapid Leak Detector
for Underground Tanks
and Pipes
                                         Principle
• Sound detection of
  vibration and elastic
  waves generated by a
  leak in a pressurized
  system by nitrogen
• Triangulation tech-
  nique to detect leak
  location

• Rapid diffusivity of
  helium
• Mix a tracer gas, with
  products at the bottom
  of the tank
• Detect helium by a
  sniffer mass spec-
  trometer

• Rapid diffusivity of
  helium
• Differential pressure
  measurement
• Helium detection out-
  side a tank
• Rapid diffusion of
  tracer gas
• Mix a tracer gas
  with product

• Detect tracer gas
  by a sniffer mass
  spectrometer using
  a vacuum pump
                                                       Claimed Accuracy
                                                           (gal/hr)

                                                       Does not provide
                                                       leak rate
                                                       Detect leak as
                                                       low as 0.01 gal-
                                                       lons per hour
                                                 Calibration
                                                 During Test
                                           Cost of
                                          Testing*
                                                                                     Does not apply   Not commercial
    Single Tank
    Preparation
      for Test

  Seal all ports
  prior to a test
                                                                                     Does not apply   By contractor
• Does not provide
  leak rate
• Helium could  leak
  through 0.005 inches
  leak size(38)
  Provide the maxi-   Does not apply   By contractor
  mum possible leak
  based on the size
  of the leak (does
  not provide leak
  rate)
  Helium could leak
  through 0.005 inches
  leak size
• Seal all ports
  prior to a test
• Monitoring holes
• Seal all ports
• Monitoring holes
  Does not  provide
  leak rate
  Tracer gas  could
  leak through
  0.005 inches  leak
  size (38)
                                                                                     Does not apply   By contractor
  Seal all ports
  prior to a test
  Monitoring holes
                                                                                                                                 (continued)

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                                                      TABLE 2  (continued)
Method
          Description
5.  Ultrasonic Leak
    Detector (Ultrasound)
6.  VacuTect (Tanknology)
7.  Varian Leak Detector
    (SPY2000 or 938-41)
                                   Principle
  Vacuum the system
  (5 psi)
  Scanning entire tank
  wall by Ultrasound
  device
  Note the sound due
  to leak by head-
  phones and register
  on a meter
• Vacuum application at
  higher than product
  static head
• Detect bubbling noise
  by hydrophone
• Estimate approximate
  leak rate by experi-
  ence

• Similar to Smith &
  Denison
  Claimed Accuracy
      (gal/hr)

Does not provide
the leak rate
A leak as low as
0.001 gallons per
hour of air could
be detected
A leak through
0.005 inches
could be
detected

Provide approxi-
mate leak rate
Similar to Smith
& Denison
                                                  Calibration
                                                  During  Test
                      Cost  of
                     Testing*
Does not apply    Not commercial
    Single Tank
    Preparation
      for Test

  Seal all ports
  Empty the tank
Does not apply    $500/tank (44)
  Seal all ports
Does not apply     By contractor
• Seal all ports
• Monitoring holes
 Charges could be negotiated with manufacturer for different numbers of tank testing and different tank specifications.

(  )See References.

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                                                          TABLE  3.   OTHER LEAK DETECTION METHODS - GENERAL INFORMATION
                                Description
                      Method
                                                  Principle
                                                     Claimed
                                                     Accuracy
                      Calibration
                        During
                        Testing
                                       Cost of
                                      Testing*
                Single  Tank
                Preparation
                 for Test
I-1
O
                       Inventory Monitoring

                       1.  Gage Stick
                       2.
                          MFP-414 TLG Leak
                          Detector
                       3.  TLS-150
                       0 Product level measur-           Gross
                         ment with dip stick
                         during station's close
                         time

                       • Product weight monitor-   Sensitive to 0.1
                         ing by pressure and      percent  of product
                         density measurement at   height change
                         the top, middle, and
                         bottom of tank
                       • Electronic level
                         measurement device
                       • Programmed micro-
                         processor inventory
                         system
Leak Effect Monitoring

 1.  Collection Sumps  •
                        2.  Dye Method
                                               Collection mechanism
                                               of product in collec-
                                               tion sump through
                                               sloped  floor under
                                               the storage tank
                       • Hydrocarbon detection
                         through perforated
                         pipe by soluble dye
Sensitive to 0.1
inches level
change
Does not provide
leak rate
Does not provide
leak rate
                                                                            No
                                                                                                  No
                                                                                                  No
                        3.  Ground  Water  and  • Water and soil sampling  Does not provide
                           Soil  Sampling                               leak rate
                        4.   Interstitial
                            Monitoring  in
                            Double-Walled
                            Tanks
                        5.   L.A.S.P.
                       • Monitoring the inter-
                         stitial space between
                         the walls of double-
                         walled tanks using
                         vacuum or fluid
                         sensors

                       • Diffusion of gas and
                         vapor to a plastic
                         material
Does not provide
leak rate
Does not provide
leak rate
                                                                                                  No
                                                                                                  No
                                                                         Does not
                                                                          apply

                                                                            No
                       Does not
                         apply
                                                                                        Minimal
                                    $5,000-$6,000
                                     (equipment
                                        cost)
                                   $5,000 (equip-
                                        ment)
                                     Provided by
                                     contractor
                                    Provided by
                                     contractor
                                    Provided by
                                     contractor

                                    By tank manu-
                                       facturer
Provided by
 contractor
                                                                                                         None
                                                                                                                               None
                                                                                                                               None
                                                                                                                               None
                                                                                                                               None
                                                                                                                               None
                                                                                                                               None
                                                                                                                               None
                                                                                                                            (continued)

-------
                                               TABLE 3 (continued)
Method
          Description
 6.  Observation
     Wells
 7.  Pollulert and
     Leak-X
 8.   Remote Infrared
     Sensing
 9.  Surface Geo-
     physical Methods
10.   U-Tubes
                            Principle
• Product sensing in
  liquid through moni-
  toring wells at areas
  with high ground water
   Claimed
   Accuracy


Does not provide
leak rate
• Difference in thermal    Does not provide
  conductivity of water    leak rate
  and hydrocarbon through
  monitoring wells

« Determine soil tempera-  Does not provide
  ture characteristic      leak rate
  change due to the
  presence of hydrocar-
  bons
11.   Vapor Wells
• Hydrocarbon detection
  by ground penetrating
  radar, electromagnetic
  induction, or resis-
  tivity techniques

• Product sensing in
  liquid
• Collection sump for
  product directed
  through a horizontal
  pipe installed under
  a tank

• Monitoring of vapor
  through monitoring
  well
Does not provide
Leak rate
                                                  Does not provide
                                                  leak rate
                                                  Does not provide
                                                  leak rate
Calibration
During
Testing
No
Does not
apply
Does not
apply
Does not
apply
No
No
Cost of
Testing*
Provided by
contractor
Provided by
contractor
Provided by
contractor
Provided by
contractor
Provided by
contractor
Provided by
contractor
Single Tank
Preparation
for Test
None
None
None
None
None
None
 Charges could be negotiated  with manufacturer for  different numbers of tank and different tank
 specifications.

-------
                                             TABLE 4.  VOLUMETRIC LEAK DETECTION METHODS - GENERAL CAPABILITIES
              Description
Method
 1.  Ainlay Tank Tegrity
     Testing
 2.  ARCO HTC Underground
     Tank Leak Detector

 3.  Certi-Tec Testing

 4.  "Ethyl" Tank Sentry
     Testing

 5.  EZY-CHEK Leak Detector
 6.  Fluid-Static (Stand-
     pipe) Testing

 7.  Heath Petro Tite Tank
     and Line Testing (Kent-
     Moore Testing)

 8.  Helium Differential
     Pressure Testing

 9.  Leak Lokator LD2000
     Test (Hunter-Formerly
     Sunmark Leak Detection)
Detects
Leak
In /Out
Both
Both
Both
Both
Both
Both
Both
Both
Both
Differentiates
Leak in Piping
or Tank
Yes
Yes
Yes
Tank Testing
Yes
Ho
Yes
No
Yes
Tests Single
or Multiple
Tanks
2
4
2
1
2
1
4
1
3
Has Potential
for Printed
Readout
No
Yes
Yes
No
Yes
No
No
Yes
Yes
Tests at
Pressure not
Greater than
5 PSIG
Yes
Yes
Yes
Yes
Yes
Yes
Sometimes No
Yes
Yes
Detects Leak
Only Below
Normal High
Fill Level
No
Yes
No
Yes
No
No
No
No
No
Total
Downtime
for Testing
10-12 hours (filled
a night before 1.5
hours testing)
4-6 hours
4-6« hours
Typically 10 hours
4-6a hours (2 hours
waiting after fill up,
1 hour test)
Several days
6-8 hours
Minimum 48 hours
3-4 hours
Requires
Empty/Full
Tank for Test
Full
No
Full
No
Full
Full
Full
Empty
Typically full
                                                                                                                                              (continued)

-------
                                                                         TABLE 4 (continued)
              Description
Method
10.  Mooney Tank Test
     Detector
11.  PACE Tank Tester

12.  PALD-2 Leak Detector




13.  Pneumatic Testing




14.  Tank Auditor

15.  Two-Tube Laser Inter-
     ferometer System
Detects
Leak
In/Out
Both

Both
Both
Differentiates
Leak in Piping
or Tank
Yes

Tank Testing
No
Tests Single
or Multiple
Tanks
3

1
1
Has Potential
for Printed
Readout
No

No
Yes
Tests at
Pressure not
Greater than
5 PSIG
Yes

Yes
No
Detects Leak
Only Below
Normal High
Fill Level"
No

Yes
No
Total
Downtime
for Testing
14-16 hours (12-14
hours waiting after
fillup, 1-2 hour test)
14 hours
14 hours (preferably
Requires
Empty/Full
Tank for Test
Full

Full
Full
Both
Both

Both
               No
Yes

Yes
 No      Try to keep below      No
           5  psi but  some
           times exceeds
               5 psi

Yes             Yes             No

Yes             Yes             No
                                                                                       a  day before,  1 hour
                                                                                      fill  testing,  include
                                                                                          sealing time)

                                                                                          Several hours
1.5-3 hours

4-5b hours
                                                                                                                   No
 Typically  full

No (at existing
     level)
alncluding the time for tank end stabilization with testing with standpipe.

''Including 1 to 2 hours for reference tube temperature equilibrium.

-------
                                             TABLE 5.  NONVOLUMETRIC LEAK DETECTION METHODS  -  GENERAL  CAPABILITIES
Method
              Description
1.  Acoustical Monitor-
    ing System (AMS)

2.  Leybold-Heraeus
    Helium Detector,
    Ultratest M2

3.  Smith & Denison
    Helium Test

4.  TRC Rapid Leak
    Detector for Under-
    ground Tanks and
    Pipes
5.
    Ultrasonic Leak
    Detector (Ultra-
    sound)
6.  VacuTect (Tank-
    no logy)

7.  Varian Leak Detector
    (SPY200Q or 938-41)
 Detects  Leak
    In/Out
   Does  not
differentiate

   Does  not
differentiate
   In  a 24-
  hour test

   Does not
differentiate
  Does not
differentiate
                              Differentiates
   In a 24-
  hour  test
Differentiates    Tests         Has          Tests at     Detects Leak
   Leak in      Single or    Potential     Pressure not    Only Below
    Piping      Multiple   For Printed      Greater      Normal High
   or Tank        Tanks       Readout      Than 5 PSIG     Fill Area
                                                     No
  Partially
                                                    Yes
                                                    Yes
  Partially
                 Several
  Partially         1


  Partially      Several
                                                                Several
                                                                               Yes
                                Yes
                                                Yes
Yes
                                                                               Yes
                                                Yes
                                                Yes
                                                                                              Ho
                                               Yes
                                                               Yes
               Yes
                                                                                            Vacuum
                                                              Vacuum
                                                               Yes
                                                                                                             Yes
                                                               No
                                                                               No
                                                               No
                                                                                                             No
                                                                               No
                                                                               No
Total
Downtime
for Testing
1-2 hours
Requires
Empty/Full
Tank for Test

No
                                                                                 None                 No
                                        Few-24 hours (exclude       Empty
                                            sealing time)

                                                 None                  No
                                                                         Few hours  (including       Empty
                                                                         tank preparation  and
                                                                           20-minute test)

                                                                                1 hour                 No
                                        Few-24 hours (exclude       Empty
                                            sealing time)

-------
                                             TABLE 6.  OTHER LEAK DETECTION METHODS - GENERAL CAPABILITIES
Method Description
Inventory Monitoring
1. Gage Stick
2. MFP-414 TLG Leak
Detects Leak
In/Out
Both
Both
LieaK in
Piping
of Tank
No
No
aingie or
Multiple
Tanks
Single
6
rotentiai
for Printed
Readout
No
Yes
treasure not
Greater
than 5 PSIG
Yes
Yes
unty oe
Normal 1
Fill Ai
Yes
Yes
    Detector



3.  TLS-150

    Tank Level Sensor

    (Veeder-Root)
                                   Both
                                                     No
                                                                               Yes
                                                                                              Yes
                                                                                                             Yes
                                                                                                                               Total
                                                                                                                                             Requires
                                                                                                                              Downtime      _  / /_ ,,
                                                                                                                            ..   „   .       Empty/Full
                                                                                                                            for Testing   _  ,   .-   _,
                                                                                                                              „   .   °   Tank  for Test
                                                                                                                              Testing
                                                                                                                             Variables          No



                                                                                                                                None            No
                                                                                                                                None
                                                                                                                                                No
Leak Effect Monitoring
                                   Out
                                                     No
                                                                Severalb
                                                                               Yesc
                                                                                         Does not apply Does not apply
                                                                                                                                None
                                                                                                                                                No
aAt the station's close of business and again at start  of day.


 Except Interstitial Monitoring in double-walled tank and U-Tubes which are used for single tank monitoring.


cExcept Dye Method.

-------
                TABLE 7.   VOLUMETRIC LEAK  DETECTION METHODS - COMPENSATION FOR EFFECTS OF VARIABLES*
2.
3.
4.
5.
Variable
;hod
Ainlay Tank
Tegrity Testing









ARCO HTC Under-
ground Tank Leak
Detector








Certi-Tec Testing








"Ethyl" Tank
Sentry Testing








EZY-CHEK Leak
Detector









Temperature
• 3 temperature
sensors
• 0.01 °F
accuracy








Not affected
by temperature
change








• 5 or more
temperature
sensors
• 0.01°F
accuracy




Thermometer
measurement at
the beginning
and end of a
test





• Averaging
temperature
coi 1
• 0.001 °F
accuracy






Ground Water
Masking
May conduct
testing when the
leak is com-
pletely masked*








May conduct
testing when
the leak is
completely
masked*






Conduct test by
standpipe if
water table is
suspected





May conduct test
while the leak
is completely or
partially masked
by variations of
the tank1 s in-
ternal forces
due to tempera-
ture and pres-
sure changes
Conduct test by
standpipe if
water table is
suspected







Tank End
Deflection
• Overnight
waiting after
tank fill up
t If tank is
filled one
hour before
testing, the
tank deflec-
tion is recog-
nized by eval-
uation of
test results
• No effect
(since the
test is con-
ducted at
normal
conditions)
• Test contin-
ues to obtain
equal leak at
two consecu-
tive tests
Recognized by
test results
evaluation






No product
delivery 24
hours prior to
a test






Recognized by
test results
evaluation








Vapor
Pockets
If the vapor
pocket is recog-
nized, the tank
top will be
excavated and
the vapor is
removed by
drilling




Not applicable










• Not applicable,
when the test
is conducted
below the fill
pipe
• Using stand-
pipe to
stabilize
vapor pocket
Not applicable









• Could be re-
leased by a
float tube
• Using stand-
pipe to
stabilize
vapor
pocket



Product
Evaporation
• Use propane
gas to reduce
evaporation
• 20-minute
testing
(short test-
ing inter-
vals)




Saturate the
vapors on top
of product
before test
by circula-
tion of prod-
uct




No compensation
when the test
is performed
without the
standpipe
(long testing)



No compensation
during 10-hour
testing







• The testing
time is short
• Overnight
testing
(usually)
• Could use
standpipe to
reduce
evaporation


Wind
Not
cora-
pen-
sat-
ed+







Par-
tial-
ly
com-
pen-
sated*





Par-
tial-
ly
com-
pen-
sat-
ed+


Not
af-
fect-
ed






Par-
tial-
ly
com-
pen-
sated
by
print-
ed re-
sult
eval-
                                                                                                                 tion*
                                                                                                           (continued)
                                                          16

-------
TABLE 7 (continued)
Vibra-
tion '

Not
conr
pen-
sat-
ed+










Par-
tial-
ly
com-
pen-
sated*
Par-
tial-
i n
ly
com-
pen-
sat-
ed+


Noise

Not
af-
fect-
ed











Not
af-
fect-
ed


Not
af-
ed





Tank
Geome-
try
• Not
corn-
pen
sated
for
temp-
era-
ture
com-
pensa-
tion
• Re-
duced
by cali-
bration*
Not af-
fected




Not com-
pensated
perature
compensa-
tion*



Instrumentation Operator
Limitation Error

Leak rate meas- Insignifi-
urement when cant
the volume
change is less
than 0.06 gal-
lons during
testing*








No limitation Insignifi-
for typical cant
tank testing
(4-inch fill
pipe)

No limitation Insignifi-
for typical cant
(4-inch fill
pipe)




Atmospheric Inclined
Pressure Tank

Not affected By cali-
bration













Not affected By cali-
bration




Not affected • Compen-
sated
when
tests
by
stand-
pipe
• Not com-
pensated
Power
Variation

Not affected














Not compen-
pensated




Not compen-
sated






when tests




below

fill pipe
Not
af-
fect-
ed




Par-
tial-
ly
corn-
pen
sated
by re-
sult
eval-
uation
and /or
by us-
ing
stand-
pipe*
Not
af-
fect-
ed




Not
af-
fect-
ed











Not com-
pensated
for leak
volume
calibra-
tion*


Not com-
pensated
for tem-
perature
compen-
sation*









• No limitation Insignifi-
for typical cant
tank testing
(4-inch fill
pipe)
f Minimum 20
inches of
product
No limitation Insignifi-
for typical cant
tank testing
(4-inch fill
pipe)










Not affected Not com-
pensated






Mot affected By cali-
bration













Not affected







Not affected














                                           (continued)
                  17

-------
TABLE 7 (continued)
Variable
Method
6.



7.





8.








9.








10.



Fluid-Static
(Standpipe
Testing)

Heath Petro
Tite Tank and
Line Testing
(Kent-Moore
.Testing)

Helium Differ-
ential Pressure
Testing






Leak Lokator
LD2000 Test
(Hunter-
Former ly
Sunmark Leak
Detection)



Mooney Tank
Test Detector


Temperature
No compensation



• One tempera-
ture sensor
• 0.003 °F
accuracy
• Product cir-
culation
Use reference
tube







• One tempera-
ture sensor
at midvolume
• 0.001 °F
accuracy
• Three temper-
ature sensors
at unusual
conditions
• Five tempera-
ture sensors
• 0.001 °F
accuracy
Ground Water
Masking
Tests by stand-
pipe


Tests by stand-
pipe




May conduct test
while the leak
is completely or
partially masked
by variation of
the tank1 s
internal forces
due to pressure
changes
May conduct
testing when the
leak is com-
pletely masked*





May conduct
testing when
the leak is
completely
masked*
Tank End
Deflection
No compensation



Stops the end
deflection
within 2 hours
by test results
evaluation

Test is con-
ducted within
48 hour s






• The end
deflection
occurs imme-
diately after
fill up
• 1.5 hours
waiting for
temperature
adjustment
Tests 12 to 14
hours after
filling

Vapor
Pockets
No compensation



The presence of
vapor pockets is
recognized by
observing
bubbles in the
standpipe
Not applicable








• Compensate if
the pocket is
released
• Not affected
during in-
tank testing



No compensation



Product
Evaporation
Not compensated



The graduate
top is capped




Not applicable








Compensated by
a hollow
sensor filled
with product





Compensated by
using an evapo-
ration cup

Wind
Not
af-
fect-
ed
Not
af-
fect-
ed


Not
af-
fect-
ed





Par-
tial-
ly
com-
pen-
sat-
ed*


Not
com-
pen-
sat-
ed*
                                                         (continued)
           18

-------
TABLE 7 (continued)
Vibra-
tion

Not
af-
fect-
ed

Not
af-
fect-
ed


Not
af-
fect-
ed

Noise

Not
af-
fect-
ed

Not
af-
fect-
ed


Not
af-
fect-
ed

Tank
Geome-
try
Not af-
fected



Not com-
pensated
for t em-
perature
compensa-
tion'1'
Not com-
pensated*



Instrumentation
Limitation

No limitation
for typical
tank testing
(4-inch fill
pipe)
No limitation
for typical
tank testing
(4-inch fill
pipe)

No limitation
for typical
tank testing
(4-inch fill
pipe)
Operator
Error

Insignifi-
cant



Insignifi-
cant




Signif icanl
potential
( inc ludtng
improper
sealing)*
                  Atmospheric   Inclined     Power
                   Pressure       Tank     Variation
                  Compensated
                  Not affected
                                                                      Not  af-
                                                                      fected
                                By cali-
                                bration
                  Not affected  Not af-
                                fected
                                           Not affected
                                           Not affected
                                                                                 Not compen-
                                                                                 sated
Par-
tial-
ly
com-
pen-
sat-
ed+
Not
af-
fect-
ed
Not com-
pensated
for tem-
perature
compensa-
tion*
Sometimes due
to tank inclin-
ation*
Insignifi-
cant
                  Compensated
By cali-
bration
                                           No t compen-
                                           sated
Not
com-
pen-
sat-
ed*

Not
af-
fect-
ed


Not com-
pensated
for tem-
perature
compensa-
tion*
No limitation
for typical
tank testing
(4-inch fill
pipe)

Insignifi-
cant




                  Not affected
                                By cali-
                                bration
                                           Not affected
                                            (continued)
                  19

-------
                                                TABLE  7  (continued)
           Variable
 Method
                          Temperature
                   Ground Water
                     Masking
                      Tank End
                     Deflection
                       Vapor
                      Pockets
                       Product
                     Evaporation
                                                                                                                  Wind
11.   PACE Tank
     Tester
12.   PALD-2 Leak
     Detector
• Three
  Thermo-
  couples

•  O.Ol'F
   accuracy

Due to short
testing time
May conduct
testing when the
the leak is
completely
masked
Tests at least
at three dif-
ferent pres-
sures
Tests 12 hours
after filling
The effect is
minimized hy
short testing
time (15 min.)
Not applicable
Must be rele
at any cost
      Compensated
      in calculation
sed   Not applicable
                                    Not
                                    com-
                                    pen-
                                    sat-
                                    ed
                       Not
                       af-
                       fect-
                       ed
14.
15.
Pneumatic
Testing








Tank Auditor






Two-Tube Laser
Interferometer
System




No compensa- May conduct test
tion while the leak
is masked com-
pletely or par-
tially by varia-
tion of tank1 s
internal forces
due to tempera-
ture or pressure
changes
Use reference The test is
tube performed at two
different levels




Use reference If the test
tube shows no leak,
the complete
masking effect
could be checked
by changing the
product level
The effect is
reduced when
the testing
time is in-
creased





Test at normal
operating condi-
tions or 3 to
6 hours after
delivery


Test at normal
operating con-
ditions




Not applicable









• Not compen-
sated during
testing in a
filled tank
• Not applicable
during in-tank
testing
Not applicable
during in-tank
testing




                                                                                                 Not applicable
                                                                                                                  Not
                                                                                                                  af-
                                                                                                                  fect-
                                                                                                                  ed
                                                                                                 • Short testing  Com-
                                                                                                 • Compensated    pen-
                                                                                                   by tempera-    sated*
                                                                                                   ture probe
                                                                                                 • Short testing  Com-
                                                                                                 • Compensated    pen-
                                                                                                   sated by       sated
                                                                                                   reference
                                                                                                   tube
                                                                                                           (continued)
                                                          20

-------
                                      TABLE 7 (continued)
 Vibra-
 tion ,
        Noise
Tank
Ge ome-
try
 Not     Not     Compensa-
 af-     af-     ted  by
 feet-   feet-   calibra-
 ed      ed      tion
Instrumentation  Operator     Atmospheric   Inclined
  Limitation       Error       Pressure       Tank
                          Thermocouple
                          accuracy
                            Insignifi-   Compensated   Not af-
                            cant                       fected
                                Power
                              Variation
                                                                                     Not affected
Not     Not    Not
com-    af-    af-
pen-    feet-  feet-
sated   ed     ed
Not     Not    Not
af-     af-    af-
fect-   feet-  fect-
ed      ed     ed
No limitation
for typical
tank testing
(4-inch fill
pipe)
No limitation
for typical
tank testing
(4-inch fill
pipe)
Significant
( inc luding
improper
sealing)*

Significant
(including
improper
sealing)*

Not affected Not compen-
sated



Not affected Not af-
fected



Not compen-
sated



Not affected




Not     Not    Cora-
corn-    af-
pen-    fect-
sated+  ed     by
               cal i-
               pen-
               sated
               bration
           Sometimes due
           to tank in-
           clination
                                           Insigni f i-
                                           cant
Not Affected  By cali-
              bration
                                                          Not compen-
                                                          sated
Com-    No t
pen-    af-
sated*  feet-
        ed
               Corn-
               pen-
               sated
               by
               cali-
               bration
           Sometimes due
           to tank in-
           clination*
                 Insignifi-
                 cant
Compensated
Compen-
sated
                            Not compen-
                            sated
 The type of liquid petroleum fuel does not affect any nonvolumetric  leak detection method  except
 the accuracy of reading of tests using "Ethyl" Tank Sentry may or may not be affected by oxygenates
 t a I "nV.nl ^
 (alcohol).
+Based on the engineering comments.
                                                          21

-------
        TABLE 8.  NONVOLUMETR1C LEAK DETECTION METHODS - COMPENSATION FOR EFFECTS OF VARIABLES*
           Variable
 Method
                     _             Ground Water
                     Temperature     ..  . .
                        r            Masking
                                                         Tank End      Vapor
                                                        Deflection    Pockets
                                                            Product
                                                          Evaporation
                                                                                                   .  ,
Acoustical Moni-
toring System
(AMS)
                       Not affected    Compensated
                                                  Not affected  Not appli-
                                                                cable
                                                          Not appli-
                                                          cable
                                                                                               Not af-
                                                                                               fected
2.
Leybold-Heraeus
Helium Detector,
Ultratest M2
                       Not affected
                                   Compensated
                                   if aware of
                                   water table
                                                  Not affected  Not appli-
                                                                cable
                                                          Not appli-
                                                          cable
                                                                                               Not af-
                                                                                               fected
3.
Smith & Denison
Helium Test
By using        Compensated
reference tube  if aware of
for leak rate   water table
approximat ion
                                                      Not affected  Not appli-
                                                                    cable
                                                                             Not appli-
                                                                             cable
                                                                                           Not af-
                                                                                           fected
4.
TRC Rapid Leak
Detector for
Underground
Tanks and Pipes
                       Not affected
                Compensated
                if aware of
                water table
                                                      Not affected  Not appli-
                                                                    cable
                                                                             Not appli-
                                                                             cable
                                                                                           Not af-
                                                                                           fected
5.
Ultrasonic Leak
Detector, Ultra-
                       Not affected
                                   Compensated
                                   by vacuum
                                                  Not affected  Not appli-
                                                                cable
                                                          Not appli-
                                                          cable
                                                                                               Not af-
                                                                                               fected
6.
VacuTect (Tank-
nology)
                       Not affected
                Compensated
                by vacuum
                                                      Not affected  Not appli-
                                                                    cable
                                                                             Not appli-
                                                                             cable
                                                                                           Not af-
                                                                                           fected
7.
Varian Leak
Detector
(SPY 2000
 or 938-41)
                   By using re-
                   ference tube
                   for  leak rate
                   approximation
                                   Compensated
                                   if aware of
                                   water table
                                                      Not affected
                                                                Not appli-
                                                                cable
                                                          Not appli-
                                                          cable
                                                                                               Not af-
                                                                                               fected
                                                                                           (continued)
                                                   22

-------
                                   TABLE  8  (continued)
  Vibration     Noise
Not  affected    Not  af-
                fected
Not  affected   Not  af-
               fected
Not  affected   Not  af-
               fected
Not affected   Not af-
               fected
Not affected   Not af-
               fected
Not affected   Not af-
               fected
Not affected   Not af-
               fected
Tank
Geometry
Not af-
fected


Not af-
fected


Not af-
fected


Not af-
fected


Not af-
fected


Not af-
fected


Not af-
fected


Instrumen- _
tatlon
T . . at or
Limita- +
Error
tion
None Signifi-
cant (in-
cluding
improper
sealing)
None Signifi-
cant (in-
cluding
improper
sealing)
None Signifi-
cant (in-
c luding
improper
sealing)
None Signifi-
cant (in-
c luding
improper
sealing)
None Signifi-
cant (in-
cluding
improper
sealing)
None Signifi-
cant (in-
cluding
improper
sealing)
None Signifi-
cant (in-
c luding
improper
sealing)
Atmo-
spheric
Pres-
sure
Not af-
fected


Not af-
fected


Not af-
fected


Not af-
fected


Not af-
fected


Not af-
fected


Not af-
fected


Inc lined
Tank
Not af-
fected


Not af-
fected


Not af-
fected


Not af-
fected


Not af-
fected


Not af-
fected


Not af-
fected


Power
Variation
Not af-
fected


Not af-
fected


Not af-
fected


Not af-
fected


Not af-
fected


Not af-
fected


Not af-
fected


 The type of a liquid petroleum fuel does not affect any nonvolumetric detection methods.

+Based on the engineering comments.
                                                 23

-------
          TABLE 9.  OTHER LEAK DETECTION METHODS - COMPENSATION FOR EFFECTS OF VARIABLES*
           Variable
 Method
                         Temperature
                                       Ground Water
                                         Masking
                                  Tank End
                                 Deflection
                                Vapor
                               Pockets
  Product
Evaporation
                                                                                                  Wind
Inventory Control:

1.  Gage Stick
2.  MFP-414 TLG
    Leak Detector
Not comp-
sated

Not affec-
ted
Not com-
pensated

By perma-
nent moni-
toring
                                                      By permanent  Not appli-   Not corapen-   Not corn-
                                                      monitoring    cable        sated         pensated

                                                      By permanent  Not appli-   Not compen-   Not af-
                                                      monitoring    cable        sated         fected
3.
    TLS-150 Tank
    Level Sensor
    (Veeder-Root)
One tempera-
ture sensor
                                       By perma-
                                       nent moni-
                                       toring
                               By permanent  Not appl-
                               monitoring    cable
                                          Not compen-
                                          sated
              Not af-
              fected
Leak Effects Moni-
                       Not appli-
                       cable
                Not appli-
                cable
                                                      Not appli-
                                                      cable
                                             Not appli-
                                             cable
                                          Not appli-
                                          cable
              Not ap-
              plicable

           (continued)
                                                  24

-------
                                     TABLE 9  (continued)
 Vibration
                                     Instrumen-
                            Tank      tation
                          Geometry    Limita-
                                       tion
Oper-
ator
Error
          Atmo-
          spheric
          Pres-
          sure
                                                                     Inclined
                                                                       Tank
  Power
Variation
Insig-
nificant
Not af-
fected
Not com-
pensated
Not af-
fected
Not com-
pensated
Not com-
pensated
Not ap-
plicable
Not com-
pensated
Not corapen-    Not ap-    Not com-   None
sated          pi icable   pensated

Not affected   Not af-    Not com-   None
               fee ted     pensated
                          for tem-
                          perature
                          compensa-
                          tion"1"

Not affected   Not af-    Not com-   None
               fected     pensated
                          for tem-
                          perature
                          compensa-
                          tion*
Not ap-        Not ap-    Not ap-    Not appli-  Not ap-   Not ap-   Not ap-
plicable       plicable   plicable   cable       plicable  plicable  p lie able
Not af-
fee ted
          Not af-
          fected
                                                                     Not com-
                                                                     pensated
                                                                                Not com-
                                                                                pensated
                                                                                Not com-
                                                                                pensated
*The type of a liquid petroleum fuel does not affect the detection methods.
 on the engineering comments.

+Based on the engineering comments.
                                                25

-------
                               SECTION 3

                              CONCLUSIONS
     The conclusions listed below are based on the review of  leak
detection methods described in this  report.

     1.   Variables affect the testing results of available or developing
         volumetric, nonvolumetric,  and in-tank monitoring methods used
         for leak detection of underground tank systems.   These vari-
         ables are potential sources of errors in using the detection
         methods successfully.  The  importance of each variable may vary
         due to the characteristics  of the tank being tested  and to such
         test conditions as the temperature of additional product used
         to fill a tank prior to testing,  depth of the water  table, tank
         deformation, random variation of  ambient temperature or pres-
         sure, tank inclination, product vapor pressure,  and  tank age.

     2.   The 36 methods identified include 15 volumetric  leak detection,
         7 nonvolumetric leak detection, 3 in-tank monitoring, and 11
         leak effects monitoring methods.

     3.   Detection methods attempt to compensate for variables affecting
         accuracy in various ways.

     4.   Available data on the performance evaluation of  the leak
         detection methods reviewed were not adequate to  determine their
         relative accuracy.
                                   26

-------
                               SECTION 4

                            RECOMMENDATIONS
     The accuracy and precision of volumetric leak detection methods
(at least) should be determined in order to permit selection of the ones
appropriate to any specific need.  A cost-effective procedure is to make
use of signal/noise theory and a high quality data base to estimate the
likely performance of each method under a variety of representative con-
ditions, and to verify performance by evaluating the method under a few,
selected, controlled conditions in a full-scale test apparatus.
                                   27

-------
                               SECTION  5

               VARIABLES AFFECTING LEAK DETECTION METHODS
     The capability of leak detection methods to accurately measure
rates of leakage is affected by variables, as well as the detection
method itself.  The principal variables and the way they affect accuracy
are discussed in this section.  This discussion of variables precedes
the description of leak detection methods in Section 6 to provide back-
ground information important to an understanding of the detection
methods.

     Principal variables which affect the accuracy of most of the avail-
able leak detection methods are:

        Temperature Change
        Water Table
        Tank Deformation
        Vapor Pockets
        Product Evaporation
        Piping Leaks
        Tank Geometry
        Wind
        Vibration
        Noise
        Equipment Accuracy
        Operator Error
        Type of Product
        Power Variation
        Instrumentation Limitation.
        Atmospheric Pressure
        Tank Inclination

The effects attributable to variables upon the ability to conduct leak
detection tests for different detection methods are discussed in this
section.  The current methods used to compensate for the variables are
discussed in Section 6 of this report.

VOLUMETRIC LEAK DETECTION TESTS

     Volumetric leak detection tests identify the leak or determine leak
rate based on the measurement of properties associated with a change in
volume.  Certain variables affect the volume change or the measurement
of the volume change.
                                    28

-------
      DRIVEWAY
MANHOLE   FILL PIPE
LIQUID IN BOTTOM
 >/2 OF TANK-590  .

   LOAD ADDED-590  :
                       3 PM        10 PM

                       61V4° ROSE TO 64°
                                               TEMPERATURE
                                                VARIATIONS
                                               AFTER FILL-UP
             3000 GAL. TANK  (64* DIA.) END VIEW
           Figure 1.   Temperature Stratification (4)


  Ref:  Heath Consultants, Inc. Petro Tite Tank Test Bulletin
                             29

-------
CM
e
    TO-
    •0-
    40'•
    10
                              _._> DAILY AMBIENT (SURFACE AIR TEMP)

                              ...... UNDERGROUND TANK

                                   . DISPENSED PRODUCT
           JPUAUJJASOMO

                                 MOUTHS





   Figure 2.  Average Gasoline Temperature  For All  Test Stations (5)



                  Ref:  API Publication  No.  4278
                                30

-------
        8

        7

        6
    £
         20*      21*       22*      23*       24*       25*

                         TEMPERATURE - °C
26°
Figure 3.  Mean Temperature Distribution As A Function Of Depth For Four
           Different 24-Hour Periods (5)

       Ref:  SRI International, Project 7637, Conducted for API
                   Technical Report 1, June 1979
                                  31

-------
                       Illlllllllltllllll
                                         ' iiiiiiiiiiiiiiim
u>
ro
                              75OOCALS
                        7OOOCALS
                        TEMPERATURE

                     SENSOR UKATIONS
                      MIOTANK

                      MIO VOLUME
                                                             e
                                                                  TIME  IN HOURS
                           Figure 4.  Tank Temperature Stratification And Gradients For A- 24-Hour

                                       Period After  Tank Fill Up  (5)
                                  Ref:  SRI International, Project  7637, Conducted for API

                                                Technical Report, June 1979

-------
  TO CHART
  RECORDER
                 AMBIENT
                        GROUND LEVa
                     SRI  UNDERGROUND TANK
                113. 5 in
                78.5  GASOLINE LEVEL  H • 85.5 in

                67.5


                44.5
                21.5
                 10.5
                 2.5
Figure 5.  Location Of Temperature Sensors In The SRI Tank (5)


  Ref:  SRI International,  Project 7637, Conducted for API
              Technical  Report 1, June 1979
                        33

-------
Temperature F
                            DELIVERY TEMPERATURES
                                                Service  Station No. 379  Houston
                                                Montrose at West Alabama
                                         Temperature of Product in Underground Tank
                          Figure 6.  Delivery Temperatures

                 Ref:  Heath Consultants,  Inc.,  Petro  Tite Tank Tester Bulletin

          Figure 6 shows the graphed  temperature recordings for an entire year by
          combining the results of  52 weekly  graphs  (4).   The vertical lines,
          either down or up, show the immediate effect of the  delivery on  the tank
          temperature and the curving lines show the gradual return  to underground
          temperatures.

          The graph also shows  a seasonal change of 30 degrees Fahrenheit  in
          underground temperatures occurring even in south Texas.  Much greater
          differences between summer  and winter would exist further  north  and
          particularly in those areas of the country noted for hot summers and
          cold winters.
         Ref:  Heath Consultants, Inc., Petro Tite Tank Tester  Bulletin

-------
Temperature

     Changes in temperature cause expansion, or contraction, in the
product and in tank dimensions.  Due to the insignificant thermal
coefficient of expansion for steel (fiberglass has a higher thermal
expansion than steel) and existence of external factors (e.g., water
table and fill material physical effects), the thermal variation of the
tank cannot be measured during the occurrence of a leak and small
temperature changes.  The product volume change can be measured because
it is much more sensitive to temperature change.  When liquid is added
to fill a tank for testing, several days may be required before the
liquid stabilizes to ground temperature; however, ground temperature is
also constantly changing (and thus prevents stabilization of the
system's temperature).  The rate of temperature change in the first day
or two after addition of liquid will generally be in the range of 0.02
to 0.25 degrees Fahrenheit per hour (3).  Temperature changes occur
because of the following conditions (Figures 1 through 6) (4,5):

        Hot days
        Cool nights
        Sunshine
        Clouds
        Rain
        Water table
        Type and compaction of fill material.

     Two important temperature effects should be considered:  volume
change and stratification.  Gasoline has an expansion coefficient of
0.00068 gallons per degree Fahrenheit (Table 10) (4).  To detect leaks
as small as 0.05 gallons per hour, a change of 0.01 degrees Fahrenheit
per hour in a 10,000-gallon tank may cause a 0.068-gallon change in the
product volume per hour, thus offsetting or amplifying an observed leak
rate.  This temperature effect could be eliminated by accurate
temperature measurement.  However, the stratification normally present
in underground tanks should also be considered.  Stratification is due
to the variation of product temperature from the top to the bottom of
the tank.  The top layer temperature may be several degrees higher than
the bottom layer.  The layer temperatures usually change at different
rates at different levels, which makes the temperature measurement more
complicated.

Water Table

     Hydrostatic head and surface tension forces caused by ground water
outside an underground storage tank may mask tank leaks partially or
completely.  Such leaks may take the form either of product leaving the
tank or of ground water entering.  When the forces are equal at two
sides of a leak opening before or during the testing period, a complete
masking effect occurs.  The chance of this situation occurring increases
                                   35

-------
         TABLE  10.  THERMAL  EXPANSION OF LIQUIDS  (4)
Ref:  Heath Consultants, Inc., Petro Tite Tank Tester Bulletin
              poonnrT                 VOLUMETRIC COEFFICIENT
      TYPE OF PRODUCT                Qp EXpANSION pER DEGREE p
Benzol (benzene)                             0.00071
Diesel fuel                                  0.00045
Ethyl alcohol                                0.00062
Fuel oil #1                                  0.00049
Fuel oil #2                                  0.00046
Fuel oil #3                                  0.0004
Gasohol
  0.10 Ethyl + 0.90 Gasoline                 0.000674
  0.10 Methyl + 0.90 Gasoline                0.000684
Gasoline                                     0.00068
Hexane                                       0.00072
Jet fuel (FP 4)                              0.00056
Kerosene                                     0.00049
Methyl alcohol                               0.00072
Stove oil                                    0.00049
Tuluol (toluene)                             0.00063
Water at 68°F                                0.000115
These are average values and may vary.  If there is any
doubt, the product should be checked with a hydrometer.
                           36

-------
when the testing method is performed on a tank which is not completely
filled and especially when no product is added or removed for testing.
The level of ground water may vary seasonally or because of intensity
and duration of rainfall.  To evaluate the masking effect, the relation-
ship between the product level inside the tank and the ground water
level outside the tank system must be known.

Tank Deformation
     Changes or distortions of the tank due to significant changes in
pressure or temperature can cause an apparent volume change in the
product.  This is called the tank deformation effect (Figures 7 and 8)
and may be affected by the wetness and nonhomogeneous properties of
backfill material around the tank (4), the material of tank
construction, the thickness of the tank shell, the age of the tank, and
forces due to ground water level exerted on the tank.  The tank
deformation effect is uncontrollable and different for every tank.

     The construction of steel tanks is such that distortion effects of
the flat ends are generally much greater than that of the cylindrical
sides (the reverse is generally true for fiberglass tanks).  The
pressure within a tank will vary with the specific gravity of the liquid
and the liquid height above the bottom of the tank.  These pressures can
be computed for any height of the tank from Table 11 (4).  The total
change of the force, in tons, at various pressure changes on each end of
a typical steel tank is shown in Table 12 (4).

     In some methods for testing tanks with large diameters, the
stabilization time for tank end deflection may be more than 36 hours.
The stabilization time for deflection of an underground tank is
important because the apparent product volume loss caused by tank end
deflection cannot be measured and may mask the occurrence of a leak.
For example, in a 96-inch-diameter steel tank, the apparent loss of
product volume is 1.957 gallons for 1/16-inch tank end deflection.  If
this volume change occurs within one hour and if it occurs during the
test period, it will offset the testing accuracy and the tank will
appear to be leaking.  The magnitude of apparent volume change for
various deflections of a given size steel tank, when it is filled, can
be found in Table 13 (4), Figure 8 (5), or can be calculated from the
following formula (4):
                                        2
                           VT  =[ f (r2+| )h][2]
                                                               *j
where V^, = total volume change due to tank end deflections, in. ,

      r = tank radius, in., and

      h = deflection of tank end, in.
                                   37

-------
                                                     Standpipa
       •Pressure  of  liquid  proportionate  to
       height  of liquid in tank  or  standpip«.
_Heod when tank it
"empty.

-Head is forced out
 in proportion to
 internal pressure
 from liquid.
                Figure  7.  Tank End  Deflection (4)

Ref:   Heath  Consultants, Inc. Petro Tite  Tank Tester Bulletin
                                  38

-------
             0.60
                                       Tank Diameters
                              64" 72" 76"  84"     96"  102"
                                NOTE:
                                   Deflection  figures  for  64"  diameter
                                   tank were measured  using  hydro-
                                   static  pressure  on  an above-ground
                                   tank.   All  other data from  tank
                                   manufacturers.
                                                I
                                                PROBABLE END DEFLECTIONS
                                                AND CAPACITY WHEN FILLED
                                                   TO GROUND LEVEL
                             Capacity, Thousand Gallons
Figure 8.  Change in Tank Volume Due To Tank End Deflections - In Gallons (5)

       Ref:  Hunter Environmental Services, Inc., Leak Lokator LD2000
                                      39

-------
Re£:
TABLE 11.  PRESSURE-HEIGHT CHART  (4),  LBS/SQ.  IN.

Heath Consultants, Inc., Petro Tite Tank Tester Bulletin
PRESSURE - HEIGHT CHART
Height Gasoline Kerosene Fuel Oil Water
1 In.
2 In.
3 In.
4 In.
5 In.
6 In.
7 In.
8 In.
9 In.
10 In.
11 In.
1 Ft.
2 Ft.
3 Ft.
4 Ft.
5 Ft.
10 Ft.
15 Ft.

Water
Gasoline
Kerosene
Fuel Oil

.026
.053
.079
.105
.132
.158
.188
.211
.237
.264
.290
.316
.632
.949
1.265
1.581
3.162
4.744
Specific
1.00
.73
.81
.85

.029
.058
.088
.117
.146
.175
.209
.234
.263
.292
.322
.351
.702
1.053
1.404
1.754
3.509
5.263
Gravity
at62°F.




.031 .036
.061 .072
.092 .108
.123 .144
.153 .181
.184 .217
.219 .258
.245 289
.276 .325
.307 .361
.338 .397
.368 .433
.736 .866
1.105 1.300
1 .473 1 .733
1.841 2.166
3.682 4.332
5.523 6.498
API Gravity
Typical
62.3) gravity
43.2) readings
35.0) varV wit^
grade and
season.
       TABLE 12.  TOTAL FORCE ON  TANK ENDS (4)
 FORMULA:  FORCE =  (AREA) X  (PRESSURE) (LBS/SQ. IN.)
               TOTAL FORCE IN TONS  AT:


 Ref:   Heath  Consultants Inc.. Petro Tite  Tank Tester  Bulletin
           Took Dio.
               1 Pti.   2 Psi.   3 Psi.   4 Psi.   5 Psi.
48"
64"
72"
84"
96"
0.9
1.6
2.0
2.8
3.6
1.8
3.2
4.0
5.6
7.2
2.7
4.8
6.0
8.4
10.8
3.6
6.4
8.0
11.2
14.4
4.5
8.0
10.0
14.0
18.0
                              40

-------
                                  TABLE 13.   APPARENT  LOSS  OF  PRODUCT VOLUME (4)
                                    DUE TO  FORCE ON TANK ENDS  - IN  GALLONS

                       Ref:   Heath Consultants,  Inc.,  Petro Tite  Tank  Tester  Bulletin
                                             APPARENT LOSS OF PRODUCT VOLUME DUE TO FORCE
                                                     OH TAMK ENDS - IN GALLONS
                                                     END DEFLECTION IN INCHES











'/..
41*

172
1 227
1 M
1 »17
121
•10»-
317

%
»•

1.74
24*
100
1*1
442
-* 12-
475

'*.
1 47

2*1
III
1M
410
J»7
**1
-» II-
1012

%
1 »i
V
14>
441
4*1
too
712
1*1 '
-1221-
1100

Vu
244
"A-
S"
111
.,,N
730
»77
ii at
-1510-
1611

%
2*1

I 22
**2
\'»
^
II 71
11.10
-II 1»-
20.1

Vu
^>

4I«
7.72
1*0
1010
1^7.
11.10
-21 40-
211

%
^
^
*.»7
1.12
*.ll
1200
ll.*l
U770
*v
-2410-
270



X-





\

%

E "1"
X
II 01
1227
1100
1*17
2220
-MM-
.1171

% 'A I 1% I'A ,.A


N










X
1*00
2110
2**0

401


"A"
"B"
x^
^s







Probable
Limit of

•21 00
2740
11 00

472



X














Limit of tank end deflection capacity
increase
Maximum tank end deflection capacity
increase

2400
si,*,
35 40"

140




X






1*10
s
"X
*07













X
4750
•/..'


























1100
. Su.l
V."








»*-

102"
120"

12*"
                                   Maximum Deflection Figures are Preliminary based on limited data
                                     from Tank Manufacturers and completely fluid soil conditions
                                        Measurements were made with air pressure above ground

-------
Vapor Pockets

     Vapor pocket effects may offset the test results obtained via
methods which require the tank to be overfilled.  This effect increases
when rapid changes in ambient pressure or temperature occur during the
test period.  Basically, three types of vapor pockets are possible:  one
that forms in the high end of a tank when the tank is not perfectly
level, one that is trapped in the top of the manway, and one that is
trapped at the top of a drop line (Figure 9) (5).  The vapor pocket may
release due to a pressure decrease or temperature increase and lead to
inaccurate leak test results. Even if the vapor pocket is not released
during the test, a change in its temperature or pressure will cause a
change in its volume, thus leading to an inaccurate test result.
Therefore, vapor pockets should be minimized, without excavations, if
feasible.  Within a short period of time, vapor pockets trapped in
abandoned lines will possibly have a significant effect, especially if
vapor pockets are close to grade and are subjected to ambient
temperature change.  As an example, for a two-cubic-foot vapor pocket at
60 degrees Fahrenheit, a 2.5 degrees Fahrenheit temperature decrease
will cause a volume decrease of 0.05 gallons.

Product Evaporation

     Evaporation causes a decrease in volume which, if not accounted
for, would be interpreted as a leak by the leak measurement device.
Awareness of this effect is particularly important in hot weather, dry
climates, and high altitudes.  The evaporation rate may differ,
depending on whether the volume change of the product is measured in or
under the fill pipe.  The evaporation rate also depends on the volume of
the empty space in the tank above the product level.  The presence of
more empty space above the product level will provide more volume for
gasoline evaporation before the space is saturated.  For example, in.a
dry climate at 70 degrees Fahrenheit ambient temperature, for a four-
inch fill pipe filled with gasoline, a rate of 0.014 gallons per hour
gasoline evaporation can be calculated by Pick's Law of mass transfer.
This is equivalent to an 0.3 inches per hour reduction of the gasoline
level in the fill pipe.

Piping Leaks

     Leaks at tank vents, manholes, or other piping connections to the
tank will cause misleading results during the leak detection tests
(because in some leak testing methods, this type of leak cannot be
differentiated from leaks which occur in the tank).

Tank Geometry

     Many of the volumetric leak detection methods are product-level
and/or temperature-sensitive.  In either case, one or more tank
specifications (e.g., the product surface area at different elevations
                                    42

-------
                                                               I
  Figure 9.  Examples Of Three Common Vapor Pockets (5)




Ref:  Hunter Environmental Services, Inc., Leak Lokator LD2000

-------
of the tank or the volume of the tank) is used to calculate the overall
volume change and the total volume change due to the temperature change
during a test period.  In either case, differences between the actual
tank specification and the nominal manufacturer's specification can
affect the accuracy of test result evaluations.

     When a reference tube filled with product is used to measure the
representative level changes due to temperature variation, the cylin-
drical geometry of the tank affects the accuracy of the test results.
This effect is minimized when the product level is at 75 percent of a
tank diameter, and increased at higher product level (33).

Wind

     When a leak detection method is sensitive to product level or
pressure changes and the fill pipe or the vents are kept open to the
atmosphere during testing, the test results can be affected by wind.
Wind, especially when it is strong, can disturb the testing and reduce
the data reading accuracy by creating a wave on the product free
surface, irregular fluctuation of the pressure exerted on the liquid, or
both.  The effect is more pronounced when the product level is below the
fill pipe.

Vibration

     In some leak detection methods, external influences such as ground
vibration, traffic, wind, and background noise may cause inaccurate test
results.  The vibration effect decreases when the testing results are
recorded based on a continuous average detection; this can be provided
by using a microprocessor.  The vibration effect in level measurement
increases as the free surface area of the product increases when the
test is conducted at product level under the fill pipe.  The magnitude
of the vibration effect is very difficult to measure precisely.  When
the test method is based on the product level measurement in the fill
pipe, the vibration may be enough to change the overall result from "not
leaking" to "leaking" (from slightly below 0.05 gallons per hour to
slightly above).

Noise

     Noise can affect the testing accuracy of a product level- or sound-
sensitive detection method.  None of the volumetric leak detection
methods are sound-sensitive.  In product level-sensitive detection
methods, the vibration due to powerful noise such as an explosion or
thunderstorm or nearby reciprocating machinery can create waves and
reduce the accuracy of the product level measurement.  Typical back-
ground noise has insignificant effect on the accuracy of nonsound-
sensitive detection methods.
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Equipment Accuracy

     Because changes of variables during a test period are commonly mea-
sured, the equipment accuracies reported by most of the manufacturers
are the sensitivity of the equipment to respond to certain variation.
However, the equipment accuracy (the ratio, multiplied by 100 percent,
of error in measurement to actual value) is subject to change at
different operating conditions such as temperature, pressure, range of
the measurement, etc.  If the variations are not compensated for during
testing, they can reduce or change the accuracy of the detection method.

Operator Error

     The more complicated the testing procedure, the greater the
potential for operator error.  Typically, this is minimized or reduced
by using trained and experienced operators to conduct the testing.  In
some cases, when the testing requires extensive sealing of the system's
ports and openings, improper sealing also could be considered as
operator error.

Type of Product

     The physical properties of the product (including effects of
possible contaminants) could affect the repeatability and/or
applicability of a detection method.  However, in all the identified
leak detection methods in this report, the accuracies are reported to be
unaffected by the type of product with physical properties similar to
gasoline.  These include jet fuel, diesel fuel, and kerosene.

Power Variation

     Most of the detection methods require electric power for oper-
ation.  In some methods, this power is provided by using batteries.
Usually, the batteries are replaced with new ones before each testing.
This reduces the testing inaccuracy due to power variation.  However,
when a method uses a 110V AC electric source, the results can be
affected by power variations during a test period.  This effect can be
reduced when both the test results and voltage measurements are printed
against a common time base and considered together during the final
interpretation.

Instrumentation Limitation

     Some of the leak detection methods are applicable to be used and
operated under certain tank  situations or operating conditions.  This
can be due to the size and range of applicability of the instruments
used in a method.  Size of a fill pipe, inclination of the fill pipe,
range of product level or pressure change are examples of variables
which can limit the applicability of a method.  If an attempt is made to
use a method outside of its  designed range, the accuracy of detection
will be decreased.
                                   45

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Atmospheric Pressure

     Barometric pressure change during a test period can affect leak
rate measurement.  For example, in a 10,000-gallon tank filled with
gasoline at approximately 60 degrees Fahrenheit (assume constant
compressibility factor) with a vapor pocket size of four gallons, a
pressure change of 0.02 inches of mercury provides an approximate
apparent leak equal to 0.0035 gallons.  However, about 80 percent of
this volume change is due to the presence of the vapor pocket (because
of the difference between the compressibilities of air and gasoline).
An apparent leak of approximately 0.01 gallons would result from a
change in barometric pressure of 0.07 inches of mercury.

Tank Inclination

     When a product level-sensitive detection method is used to
determine leaks in an underground storage tank, tank inclination can
affect detection accuracy.  In an inclined tank, the volume change per
unit of level change is different than in a horizontal tank.  This is
due to the difference between cross sectional areas, at certain product
elevations, for inclined and vertical conditions.  This effect is
corrected by measurement of level change due to a known product volume
change.

     In some cases, significant inclination may cause the method to be
inapplicable.

NONVOLUMETRIC LEAK TESTS

     The nonvolumetric  leak detection test is used to determine the
presence of leaks by qualitative analysis, usually by using a second
material other than the product (tracer material).  The performance of
testing may be affected by certain  variables.

Temperature

     If a  tank must be  emptied and  then filled  with a tracer material
 (usually helium)  prior  to leak testing, the  temperature effect can
 change  the pressure and the viscosity of the  tracer material.  The  leak
 rate of tracer material will  increase with temperature  increase.  This
 is  the  result of  pressure increase  and viscosity  decrease of a tracer
 material due  to  temperature  increase, both of which tend  to  increase  the
 leak rate.  However,  because  the  typical tracer material  is  helium  with
 significant diffusivity,  the  temperature increase can only  reduce  the
 detection  time of the  tracer  slightly.  Therefore,  the  accuracy  of  this
 test  is not significantly affected  by temperature changes.

      Some  detection methods,  in  addition to  detection of  leaks  by  tracer
 gas,  attempt  to  provide an  approximate  leak  rate  by pressure monitoring
                                    46

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during a test period.  These methods must compensate for pressure change
due to temperature effect.

     If testing is conducted with product at normal existing conditions
and leaks are detected by monitoring the sound due to leaks or detection
of tracer gas outside a tank, the change of the leak rates due to
temperature change will have slight effect on the detection time and no
effect on the testing accuracy.

     The change of the temperature would be based on ambient temperature
change, sunshine, clouds, rain, water table, and type and compaction of
backfill material.

Water Table

     If a detection method indicates a leak by detection of tracer gas
outside of a tank, the presence of a high water table can prevent the
exit of the tracer gas from the tank.  However, this can be overcome by
increasing the pressure of the tracer material inside the tank until it
exceeds the external pressure, in which case the tracer gas (helium)
will bubble up through the water to the surface.  For certain pressure
of tracer material inside the tank, a higher water table will result in
a longer detection period.

     Some detection methods, in addition to the detection of leaks by
sniffing tracer gas outside a tank, attempt to provide maximum possible
product leak rate by'pressure monitoring inside the tank.  In this case,
a partial masking effect of the water table affects the testing accuracy
for leak rate evaluation.

     When a method is applied to detect leaks by sound monitoring of the
leak under pressurized or vacuumed tank conditions, a lower partial
masking effect (lower water tables) can cause a more pronounced sound
for detection of a leak.  In this case, due to the pressure differential
at two sides of a leak opening, a complete masking effect is avoided.

Tank Deformation

     The nonvolumetric methods operate either by monitoring a tracer gas
outside a tank or monitoring the sound due to a leak inside a tank.
Therefore, tank deformation does not affect the detection accuracy.
(However, the effect of the tank deformation on the diameter of small-
size leaks should be studied.)

     When a method provides the maximum possible leak rate of the
product by pressure monitoring inside a tank, the tank end deflection
effect on the leak rate will decrease for longer test periods.
                                   47

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Vapor Pocket

     In nonvolumetric detection methods it is necessary to test a tank
at emptied or normal existing product level condition.  Therefore,
during these testings, vapor pockets cannot be created.

Product Evaporation

     When testing is conducted on a completely empty tank, the product
evaporation effect is eliminated.  If a nonvolumetric method indicates
leaks by detection of a tracer gas outside a tank or sound monitoring of
leaks inside a tank, in both cases at normal existing product level, the
product evaporation cannot affect testing performance.

Piping Leaks

     In nonvolumetric tank leak testing with tracer gas, leaks at tank
vents, manholes, or other piping connections to the tank can cause
misleading results.  This is because the tracer gas is very diffusive
and can diffuse through some pipe connections even after they are
tightened enough to contain liquids.

Tank Geometry

     None of the nonvolumetric leak detection methods is product level-
sensitive.  Therefore, tank geometry does not affect testing.

Wind

     Based on the testing procedures for nonvolumetric detection
methods, all the ports of a tank should be sealed from the atmosphere
prior to testing to assure that the wind does not affect the testing
performance.  However, in some detection methods where leak detection is
performed by sniffing a tracer gas at the ground level above a tank, in
windy conditions, small monitoring holes should be installed.  This will
prevent the masking effect of wind for detection of tracer gas by direct
sniffing of gas through monitoring holes.

Vibration

     None of the nonvolumetric detection methods are sensitive to the
level change of any fluid during a testing period.  Therefore, the
testing performance is not affected by the vibration effect.

Noise

     Noise can affect the testing accuracy of a sound-sensitive de-
tection method.  Unless the background noise can be differentiated from
the sound due to leaks, the test cannot be successfully carried out.
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Equipment Accuracy

     (See the description for volumetric leak detection methods.)

Operator Error

     In all nonvolumetric methods, all tank ports must be sealed from
the atmosphere.  Therefore, one of the major potentials for operator
error is the operator's ability to seal a tank completely prior to a
test.  In sound-sensitive detection methods, the operator's level of
experience can reduce the time required to assure the certainty of
detecting leaks or the leak rate.

Type of Product

     When testing is performed in an empty tank, the effect due to type
of the product will be completely eliminated.  In acoustical leak
detection methods which are conducted in tanks containing product, the
product viscosity can affect the sound characteristics of leaks below
the product level.  However, for products with properties similar to
liquid petroleum fuel, this effect is insignificant.

Power Variation

     The nonvolumetric leak detection methods are based either on
detection of a tracer gas  (helium) outside the tank or detection of the
leak sound inside a tank.  In either case, the typical AC power
variation during the detection period cannot be enough to mask the
detection completely.

Instrumentation Limitation

     (See the description  for volumetric leak detection methods.)

Atmospheric Pressure

     Because all the nonvolumetric detection methods are operated only
after the tank ports are sealed  to the atmosphere, atmospheric pressure
(barometric pressure) change has no effect on the test results.

Tank Inclination

     Because none of the nonvolumetric leak detection methods are
product-level  sensitive, tank inclination does not affect testing.

General  Problems

     The principal  problems  inherent  in nonvolumetric detection methods
are  that  they:
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     •  Cause or enhance a Leak during testing by exerting pressure
        higher than normal tank operating pressure.

     •  Adversely affect product quality if a compound that is not inert
        is used for testing in a tank containing product.

     •  Risk an explosion hazard when product is present in the tank
        during testing.

     •  Usually cannot measure leak rate accurately,  or at all.

     •  Require a long testing time for low leak rates when the type and
        compaction of the backfill  material around the storage tank is
        varied.  In some cases, the testing time could be  up to 24
        hours.

INVENTORY CONTROL

     The problem of keeping records of product inventory is complicated
by the fact that gasoline is volatile and losses due  to evaporation are,
to a degree, unavoidable.  However, the inventory method could be used
as a first and most convenient method for gross leak  monitoring.  The
accuracy of this method is very much related to the manner in which
variable factors are compensated.

LEAK EFFECTS MONITORING

     Problems associated with methods in this category are not discussed
in this section because these methods are not considered as existing or
developing in-tank, leak detection  techniques, which  are the focus of
the present study.
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                               SECTION 6

                     LEAK DETECTION METHODS REVIEW
     All leak detection methods discussed are reviewed in this
section.  The classifications of leak detection methods are presented
first,  and then the methods themselves are described.  Tables 1 through
9 (in Section 2) summarize the general information and operational
capabilities for each of the leak detection methods discussed in this
report.

     Note that each "Manufacturer's Description of Method" is based on
the available literature from the manufacturer of that method.  However,
the information regarding the "Manufacturer's Techniques to Compensate
for Effects of Variables" is a combination of the available information
in the manufacturer's literature, reports, and/or verbal communications
with the staff of the manufacturer.

     The "Engineering Comments" herein are based on the authors' engi-
neering 'judgment .  Therefore, it is possible an engineering judgment
would be different from the information or detection method capabilities
claimed by the manufacturer.

     As used in this section, "testing" refers to those leak detection
methods that determine, at a point in time, whether a tank or tank
piping is tight or leaking.  Testing is different than monitoring
techniques.  Monitoring techniques provide continuous surveillance to
detect early leaks or area-wide surveillance to investigate the source
of a leak or spill.  "Tank testing" refers to the detection of leaks in
tanks and tank piping systems.

CLASSIFICATION

     The four general classes of methods to detect leaks in underground
storage tanks are:

     •  Volumetric (quantitative) leak testing, for leak indication and
        leak rate measurement

     •  Nonvolumetric (qualitative) leak testing, for leak indication

     •  Inventory control
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     •  Leak effects monitoring. ^

These methods can be used individually or in combination.

Volumetric (Quantitative) Leak Testing

     This classification of testing includes methods which test for
leaks based on the volume change.  The change in volume can be deter-
mined by measuring parameters associated with volume change; including
changes in liquid level, temperature, pressure, and density.

Nonvolumetric (Qualitative) Leak Testing

     This classification of testing includes methods which principally
determine the presence of a leak in an underground storage tank by
qualitative measurements.  After identifying an underground tank leak by
this technique, a volumetric test can be used to measure the leak rate.

     The main concerns about most qualitative testing methods are:
potential enhancement of leak, effect on product quality, explosion
hazard, inability to measure the leak rate, and required time for
testing.

Inventory Control

     Advocates of inventory control claim it is the simplest and most
economical leak detection method.  They contend that the technique has
not worked in the past only because recommended practices have not been
followed.  Recommended practices for inventory control at service
stations can be found in the American Petroleum Institute's Publication
API 1621, Recommended Practice for Bulk Liquid Stock Control at Retail
Outlets (55).

Leak Effects Monitoring

     This classification of leak detection methods identifies leaks by
monitoring the environmental effects of the leak inside or outside an
underground  storage tank.  These methods usually require drilling small
holes  or wells, installing monitoring casings, and chemical analysis.

LEAK DETECTION TESTING METHODS

Volumetric (Quantitative) Leak Testing Methods

1-  Ainlay Tank Tegrity Testing  (TTT)  (6,7)—

     Manufacturer's Description  of Method (6)—In this method,  the level
change in a  completely filled tank is measured by monitoring pressure
change through a  bubbling  system (Figure 10).  The method is used to
measure and  differentiate  leaks  in tank and piping.  The tank is  filled
into  the  fill  pipe  the evening  before testing.
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Air and water chamber
wrapped around with
plastic tubing makes
a Manometer
Hose to bubble tube
                                                Digital
                                                Thermometer
                                                Sensitive to
                                                 .005°  F.

                                                Bubble tube
                                           Thermometer probes
            Figure  10.  Ainlay  Tank  Tegrity  Testing  Method

            Ref:  Schematic Drawing  by  Steel Tank Institute
                                 53

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     Propane gas bubbles are introduced one inch below the product level
through a 1/4-inch copper tube.   The pressure required to introduce
bubbles varies with changes in product level, and is related to volume
changes.  Pressure changes are monitored by a manometer type coil (slope
tube) with a colored water indicator.  A slight drop in liquid in the
tank is exaggerated approximately 50 times when transmitted from bubble
tube to the slope tube.  The temperature change during the test period
is measured.  Based on data available at the site on tank volume, the
volume change due to temperature change during a test period is calcu-
lated.  Finally, the volume change due to a leak is calculated by
subtracting the volume change due to temperature change from the total
volume change.

     Ainlay TTT can be performed in one hour and can detect a leak as
small as 0.02 gallons per hour.   The equipment used for setup and
operations is carried in a portable case and can be hand carried as
baggage on board an airplane.

     Manufacturer's Techniques to Compensate for Effects of Variables
(7)—In the Ainlay TTT detection method, the following effects of
variables are compensated for as described below:

     •  Temperature—Temperature change is measured by three electronic
        temperature probes at the center of each of three product layers
        with 25 percent, 50 percent, and 25 percent, respectively, of
        tank volume.  Locations of the probes for tanks with various
        diameters are provided on a table.  When the three temperature
        readings have stabilized, the temperature reading is recorded
        and averaged on the report form.  The temperature can be read on
        a digital display with 0.01 degrees Fahrenheit accuracy.

        The API gravity of the product is measured at the beginning.of
        the test with a hydrometer.  A table is included in the
        instruction book.  For testing a tank, this table will translate
        the API gravity reading to coefficient of expansion.  This table
        covers all petroleum products from fuel oil to highest API
        gasoline.  Since the coefficient of expansion of chemical
        solvents cannot be determined by hydrometer, another table is
        included to cover 175 chemicals such as alcohol, acetones, etc.

        If the tank tested has a drop tube (an insert in the fill pipe
        which extends nearly to the bottom of the tank), it must be
        removed before the test because the tube affects accuracy in the
        detection of temperature shifts.  In addition, filling and
        allowing the tank to stand overnight stabilizes the temperature
        in advance of the test.

      •  Water Table—The presence and amount of water in the tank is
        determined with water-finding paste on the depth level stick at
        the beginning and completion of the test.  An increase or
                                   54

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   decrease in the water Level will indicate a Leak into or out of
   the tank.

•  Tank Deformation—This effect is minimized by filling the tank
   the evening before testing (8).  However, if the tank is topped
   off one hour before the test, the end deflection effect is rec-
   ognized when the calculated leak rates change in a decreasing
   manner.  As long as the end deflection is recognized and the
   measured volume changes are not correlated with changes caused
   by temperature change, the calculated leak rate is not con-
   sidered as TTT's final result.  Therefore, the overall testing
   time will increase.

•  Vapor Pockets—If vapor pockets are noticeable, the suspected
   locations are excavated and the vapor pocket is released (8).
   (For example, the vapor pocket at the end of the tank is
   released by drilling a hole at that end.)  As a second alterna-
   tive, the test is conducted when the level of the product is 0.5
   inches under the fill pipe.

•  Product Evaporation—Propane gas is bubbled into the tank to
   reduce the evaporation due to bubbling of gas in the product.

•  Piping Leaks—A leak in the piping system can be detected by
   lowering the product level to about one inch into the fill pipe,
   or one inch above the top of the tank.  This places the product
   level below the piping level.  If a leak is indicated at this
   level, it must be in the tank as lines are not involved in the
   test.

•  Equipment Accuracy—Digital temperature probes register and read
   out temperature shifts as small as 0.01 degrees Fahrenheit.  The
   volume change of approximately less than 0.01 gallons can be ob-
   served on the manometer (slope tube).

•  Operator Error—As operator skill increases, the temperature
   reading can be as precise as 0.005 degrees Fahrenheit.  In
   addition, a better estimation of a portion of a 0.01-gallon
   volume change can be provided.

•  Type of Product—As long as a bubble can be generated in the
   product, the accuracy of the TTT method does not change (8).

•  Tank Inclination—This effect can be corrected by measuring the
   exact product volume change in the coil-type manometer with
   change in product level in the fill pipe.  This is done by
   addition/removal of the product, with known volume, to/from the
   fill pipe until the product level in the slope tube reaches the
   level when the test began.
                              55

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     •  Tank geometry,  noise,  power variation, and atmospheric pressure
        do not have an  effect  on testing accuracy (8).

     Engineering Comments—The Ainlay TTT's accuracy may be affected for
the following reasons:

     •  Differences between measured temperature changes and actual
        temperature changes.

     •  Lack of compensation for masking effect on the leak rate caused
        by hydrostatic  pressure and surface tension.

     •  Presence of unidentified vapor pockets.

     •  Evaporation of  product during a test.

     •  Difference between the obtained tank volume and the actual
        volume.

     •  Strong wind.

     *  Strong vibration.

     •  Slope tube limitation  to measure volume change more than 0.06
        gallons during  the test.

     •  Effect of barometric change on vapor pocket volume (if any).

In addition to the above, another disadvantage of this method is that a
printed readout is not  provided for studying unusual events during a
test.

2- ARCO HTC Underground Tank Leak Detector (7,9,10,11,12)--

     Manufacturer's Description of Method (7,12)—The ARCO underground
tank leak detector is an ultrasensitive device for measuring volume
changes in an underground storage tank caused by leaks through tank
walls under a product level, or product distribution lines (Figure
11).  This method is substantially unaffected by temperature changes
that may occur in the tank during a test.  However, a one-hour waiting
period is recommended to allow the equipment to stabilize and wave
action to diminish.  To minimize fuel evaporation during the test
period, a saturated vapor condition is provided above the liquid
phase.  This is done by circulating the fuel in the tank for an amount
of time, set by tank size.

     The ARCO system consists of a float, a detector rod, and a strip
chart recorder.  The float senses the liquid level in the tank, the
detector rod measures the relative position of the float with respect to
the rod, and the recorder makes a permanent record of the measurement.
Figure 11 illustrates the arrangement of testing equipment in a tank.
                                   56

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                                             • Height Adjustment

                                                  Tank Riser

                                                  3/8" Pipe
                                                  (Detector Rod)
                                              DETECTION DEVICE
  Linkage
Hollow Tube
         Figure 11.  ARCO Underground Tank Leak Detector (12)

          Ref:   ARCO Underground Tank Leak Detector Bulletin
                               57

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     The float is assembled differently for different tank types.  A
float shell is selected from a group of varying length shells suitable
for a variety of tank sizes.  The float length and weight are chosen
based on the tank diameter, the liquid height in the tank, and the
liquid density.  These measurements are taken at the site just prior to
starting the test.

     The detector rod assembly consists of a photoelectric cell and a
float attachment hinge.  The float movement forces an ink-type solution
into or out of the photocell.  The change in light transmittance in the
photocell results in a voltage drop across the cell.  The voltage
change, which is a function of the product level change, is measured by
a precalibrated voltage meter.  Calibration and one-hour testing periods
are continued until two consecutive readings give the same calculated
result.  The strip chart recorder has multiple input ranges.  The ARCO
system can test four tanks simultaneously.

     The test can be performed accurately when the tank level is between
66 and 76 percent of the tank diameter (9).  Only leaks under the
product level may be detected.

     The ARCO leak detector can be used with the tank at a normal opera-
ting level and pressure.  The entire test procedure takes two to three
hours and leaks smaller than 0.05 gallons per hour can be detected;
however, longer test periods are possible.  Operator attendance  is not
required during each one-hour test interval.

     Manufacturer's Techniques to Compensate for Effects of Variables
(7,12)—In the ARCO Tank Leak Detection testing methods, the following
effects of variables are compensated as described below:

     •  Temperature—The detector takes advantage of natural temperature
        compensation by selecting a point in the tank (when the  product
        level  in  the tank  is  less than 76 percent of tank diameter)
        where  a floating object will be unaffected by temperature
        variations in  the  liquid.  A relationship exists between
        temperature and three factors; namely, liquid density, liquid
        buoyant forces  (a  function of density), and  liquid volume.  A
        change  in temperature, affecting  liquid volume, can be exactly
        offset  by density  (buoyancy) changes, providing the floating
        object  is at the point where the  volumetric  and density  changes
        caused by temperature variation have an equal, neutralizing
        effect.

      •  Water  Table—Water ingress will be  detected  as an upward float
        movement, thus the ARCO  system detects  "leaks in" as well  as
        "leaks out."

      •  Tank Deformation—Because  the  tank  is not overfilled  during  the
        test,  no  provision needs  to  be made for this  effect.
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     •  Vapor Pockets—Vapor pockets are not formed in this test
        (because the tank is not filled).

     •  Evaporation—Based on field observation,  this method reduces
        product evaporation during the test period by providing a
        saturated vapor condition above the liquid phase.  This is done
        by circulating the product in the tank for a required period
        before conducting the test.

     •  Piping Leaks—When the tank testing is complete,  the submerged
        pump (which is part of the tank system) is turned on, and the
        dispenser is kept in the off position; therefore, leaks in the
        lines are measured with this method.

     •  Tank Geometry—In a horizontal cylindrical tank,  the thermal
        effect on level change is minimized when  the product level is as
        described in the test procedure (13).

     •  Equipment Accuracy—The system is calibrated for  readout for
        level change due to one liter volume change at the beginning of
        each one-hour test.

     •  Operator Error—The operator error will be reduced with train-
        ing, experience, and follow-up of the  testing procedure (12).

     •  Type of Product—The method could be used with any type of
        liquid as long as the float can move freely (12).

     •  Tank Inclination—The effect due to this  variable is compensated
        by using a calibration at the beginning of each one-hour test.

     •  Noise, power variation, and instrumentation limitation will not
        affect the testing accuracy (12).

     Engineering Comments—The accuracy of the testing may be affected
for the following reasons:

     •  Existence and change in the water level at the bottom of the
        tank. This prevents a constant buoyancy force during the test
        period.  In addition, leak rate reduction or masking due to
        ground water cannot be avoided.

     •  Occurrence of waves on the product's free surface due to wind
        and vibration.  However, this effect is partially corrected by
        the chart results evaluation.

     •  Power variations.

     •  Atmospheric pressure change during the test period.
                                   59

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     In addition, one of the disadvantages of this method is that tank
leaks above the product Level will be undetected.

3- Certi-Tec Testing (10,14)—

     Manufacturer's Description of Method (14,15)—The Certi-Tec test
monitors pressure changes resulting from product level changes (Figure
12).  Product level changes are due to volume changes.  The method is
capable of testing storage tanks filled either beyond or below
capacity.

     The system uses a sensitive pressure transducer located below the
product surface.  Five or more temperature sensors are used to measure
temperature at different levels.  A microprocessor collects temperature
and pressure change data and determines the volume change of the mass
above the pressure transducer.

     When it is possible to fill the tank, the test method uses a stand-
pipe.  The standpipe is installed above the grade of the tank.  The
pressure transducer is installed in the standpipe and the product level
change is measured.  If a leak is detected, the product level is
decreased below the fill pipe and the pressure transducer installed in
the tank.  The results of the tests at these conditions could determine
if the leak is in the tank or piping.

     The system accuracy to measure leak rate is within that recommended
by NFPA (0.05 gallons per hour).  The accuracy of the test is reduced
when a partially filled tank is tested.  However, to achieve maximum
accuracy, the test must be performed over a longer period of time than
the test with the standpipe.  The test can be performed in two- to four-
hour testing periods.

     Manufacturer's Techniques to Compensate for Effects of Variables
(15)
—In the Certi-Tec Tank testing method, the effects of the following
variables are compensated as described below:

     •  Temperature—In this system, temperature sensors are suspended
        at five  or more levels.  A microprocessor collects the tempera-
         ture data to measure the volumetric average of product tempera-
         ture during a  test.  The volume change of the mass above a
         pressure transducer, which is used for leak detection, is
         determined  for  the estimated temperature change  (10,14).

     •   Water Table—A potential problem exists when  the test is con-
         ducted  in a tank  filled with less  than capacity  and  the  tank  is
         located  in high ground water conditions.  The ground water could
         mask  the leak.  In  this testing,  the level of water  in the tank
         is measured by water-finding paste.
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DATA LOGGER
n
— | 	 1 1— 1 ^ TO 110 V POWER SUFFLJ


3
1 	 1 II 	 '
PRESSURE TRANSDUCER POWER SUPPLY V\
LIQUID LEVEL ^
PRESSURE TRANSDUCER
j FILL PIPE
                               UNDERGROUND STORAGE TANK
Figure  12.   Certi-Tec Tank  Testing System  (14)




 Ref:   Schematic Drawing  by Fuel Recovery  Co.
                      61

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     •  Tank Deformation—This effect  is recognized when  the measured
       leak rate changes in a decreasing manner.

     •  Vapor Pockets—When a tank can be filled, a test  is conducted
       with standpipe.  In this case, the head  pressure  induced  by  the
       standpipe can  reduce the vapor pocket volume  (if  any)  and,
       therefore, reduce the volume change due  to vapor  pocket
       effect.  When  the test is conducted with product  level under the
       fill pipe, no  vapor pocket exists to affect the testing accur-
       acy; however,  this reduces the pressure  transducer sensitivity
       and increases  the time for testing.

     •  Equipment Accuracy—The temperature readout of smaller than  0.01
       degrees  Fahrenheit can be recorded.  In  addition, the  pressure
       transducer can provide ±0.25 percent accuracy and ±0.05 percent
       repeatability.

     •  Operator Error—Operator error will be minimized  if the testing
       procedure is followed precisely.

     •  Type of  Product—The system could be used with gasoline,  jet
       fuel, diesel fuel, and other liquid petroleum fuels.

     •  Instrument Limitation—The pressure transducer can only be used
       from 0  to 3  pounds per square  inch pressure range.

     •  Atmospheric  Pressure—The  system is designed  to compensate  for
       atmospheric  pressure change during the test period.  This is
       accomplished by measurement of the gage  pressure.

     •  Noise and power variations will  not affect  the test results:

     Engineering Comments—The accuracy  of the Certi-Tec  testing  can be
affected  by:

     •  Difference  between measured  temperature  changes and actual
        temperature  changes.

     •   Lack of compensation  for  water table masking  effect or reduction
        of the  leak rate.

     t  Vapor pockets, if  the  test  is  conducted  using the standpipe.

     •   Product evaporation  when  the  test is  conducted without
        standpipe.

     t   Difference  of  obtained tank volume with  the actual  volume.
                                   62

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     •  Wind,  especially when the test is conducted at product level
        below the fill pipe.  However, it is partially corrected by the
        microprocessor, which continuously provides the average results
        for every 15 seconds.

     •  Vibration, especially when the test is conducted at product
        level  below the fill pipe.  However, it is partially corrected
        with the same technique to compensate for wind.

     •  Equipment accuracy should be checked for each test by
        calibration.

     •  Power variations.

     •  Effect of atmospheric pressure change on vapor pockets volume
        (if any).

     •  When the test is conducted with a pressure transducer in the
        fill pipe or tank, the tank inclination effect should be
        compensated by calibration.

4-"Ethyl" Tank Sentry Testing (7,9,10,11,16) —

     Manufacturer's Description of Method (16)—The "Ethyl" tank sentry
is used to detect and measure small changes in the liquid level of
underground fuel tanks.  The heart of the detector is a "j" tube man-
ometer containing a special indicator fluid; the fluid is not miscible
with fuel.  The long leg of the "J" tube connects with a larger diameter
fuel reservoir.  A manually operated valve on the long leg of the "J"
tube is used to admit or drain fuel from the reservoir.  A second valve
is installed in the short leg of the "j" tube to control the indicator
fluid.  Both valves can be operated while the detector is in the tank.
Figures 13 and 14 illustrate the detector kit and the installation of
the detector in a tank (16).

     The operating principle during the test is that a change in the
indicator fluid level occurs due to a change in the liquid level of a
partially filled tank.  Any change in tank level is magnified by a
factor of approximately five in the manometer.  The difference in height
of the indicator fluid in the manometer legs is read and recorded.  By
referring to tank tables and applying certain factors, the loss or gain
in fuel volume is calculated.  A level change as small as 0.02 inches
can be detected.  For a one-hour test with the product level in the
middle of a typical, cylindrical 8,000-gallon tank (eight-foot
diameter), a change of 0.02 inches per hour reflects a leak rate of 2.12
gallons per hour.  Because the accuracy in measuring and detecting leaks
is a function of the time span of the test, the probability of detection
can be increased by extending the test time or by averaging two or more
replicated tests.  As an example, a level change of 0.02 inches within a
ten-hour span (instead of a one-hour span) calculates to a 0.212 gallons
                                   63

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Figure 13.  "Ethyl" Tank Sentry Kit (16)




      *   Ethyl Corporation Bulletin
                          WATER TRAP
Figure 14.  «Ethyl» Tank





       Ref:  Ethyl Corporation Bulletin
          64

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per hour leak rate.   The test requires that the test period must span
several hours.

     Manufacturer's  Techniques to Compensate for Effects of Variables
(17)
—In the "Ethyl" Tank. Sentry testing,  the following effects of variables
are compensated as described below:

     •  Temperature—The temperature is measured by a temperature probe
        (thermometer).  This is done before and after the tests and is
        used to calculate the volume change due to temperature effect.
        Equipment instructions state that a one degree Fahrenheit change
        in product temperature during the test will negate the results;
        tests should not .be conducted within 24 hours after product
        delivery.  After this time,  the product temperature usually
        varies less  than one degree  Fahrenheit for the test period.  In
        addition, careful adherence  to the test procedure reduces
        possible effects of temperature variables (16).

     •  Tank Deformation—This effect is eliminated during the testing
        period.  This is due to the  test requirement that the tank be
        idle and no deliveries be made to the tank during the preceding
        24 hours.  In addition, careful adherence to the test procedure
        reduces possible effects of  tank end deflection variable (16).

     •  Vapor Pockets—Because the testing requires product level under
        the fill pipe, this effect is eliminated

     •  Noise—Not applicable.

     •  Equipment Accuracy—Any change in tank level is magnified in the
        manometer, making it possible to detect level changes as small
        as 0.02 inches.

     •  Operator Error—This can be minimized by carefully following the
        testing procedure.

     •  Type of Product—The testing accuracy would be unaffected by the
        product type as long as the viscosities and vapor pressures of
        products are not too high.  However, "Ethyl" Tank Sentry may or
        may not give accurate readings with gasolines that contain any
        oxygenates (alcohol).

     •  Power Variation—Not applicable.

     •  Instrumentation Limitation—The method is used to measure leaks
        in underground fuel tanks having a three-inch or larger fill
        pipe diameter and containing at least 20 inches of fuel (16).
                                   65

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     •  Atmospheric Pressure—The manometer eliminates the effect of
        barometric changes during the testing period.

     Engineering Comments—The "Ethyl" tank sentry testing accuracy may
be reduced due to the following reasons:

     •  Difference between measured temperature changes and actual
        temperature changes.

     •  Lack of compensation for water table level on the leak rate.  In
        addition, it is not capable of preventing masking effect due to
        the water table.  However, the effect is reduced when a test is
        conducted for a longer period of time.

     •  Product evaporation during the test period due to the tempera-
        ture and/or pressure change.

     •  Piping leaks.

     •  Difference in the calculated surface area and volume of the pro-
        duct, based on the available tank's data, and the actual values
        to estimate the overall volume change and thermal volume change
        during a test period.

     •  Tank inclination is not considered or compensated by
        calibration.

In addition, the system disadvantages include:

     •  The data are not recorded continuously.  They are only recorded
        at the beginning and end of the test period.

     •  The leaks are not detected above the product level in the
        storage tank.

     •  Long testing period is required to differentiate between tank
        leaks and piping leaks.  Therefore, usually another method of
        leak detection is required for pipe testing.

5- EZY-CHEK Leak Detector (5,7,10,11,18,19)—

     Manufacturer's Description of Method (5,18,19)—In this method, the
level change is measured by monitoring the pressure change through a
bubbling system.  The storage tank is typically overfilled into the fill
pipe. However, the testing can be taken at any level in the standpipe
above the highest point in the tank, in the fill pipe, or in the tank.

     The system consists of a standpipe, an averaging temperature probe,
an air supply tank and chart recorder.  The liquid level change is
monitored with a sensitive pressure gage.  The pressure recorder has a
                                   66

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Figure 15.  Ezy-CHEK Leak Detector (18)




 Ref:  Horner Creative Metals Bulletin
                   67

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       Figure 16.   EZY-CHEK Leak Detector Installation (18)'

              Reft   Horner Creative  Metals Bulletin
                         EXTEND OR
                         CONTRACT TO
                         MONITOR TEMP
                         CHANGE FROM
                         TO BOTTOM
                         OF TANK
Figure 17.   EZY-CHEK Leak Detector Temperature Averaging Probe (18)

               Ref:  Horner  Creative.Metals  Bulletin
                                  68

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full range of approximately one ounce of pressure.   The air supply
forces a small flow of low pressure air into the top 1/2 inch of liquid
in the tank,  through a 1/4-inch tube clamped to the fill pipe.  The
recorder measures the pressure necessary to cause the bubbling action.
If the recorder charts a straight line, the liquid  level is not chang-
ing.  The temperature change is monitored with an averaging temperature
probe to compensate for the volume change due to the temperature vari-
ation during  the testing period.  Figures 15 through 17 illustrate the
equipment and the installation of the EZY-CHEK system (18).

     Complete tank testing includes at least four 15-minute testing
periods and could usually be performed with 0.01 gallons per hour leak
detection accuracy within four hours after the tank is topped off.

     Manufacturer's Techniques to Compensate for Effects of Variables
(5,18,19)—In the EZY-CHEK testing method, the following effects of
variables are compensated as described below:

     •  Temperature—Temperature change is monitored by an electronic
        temperature averaging probe which is installed in the tank.  The
        probe consists of platinum sensing wires encased in a "coil
        spring" of special plastic tubing.  The probe is formed with
        more coils at the center of its length than at its ends, thus
        proportioning the length of sensing wire to the volume of the
        tank.  When the weighted probe is dropped into any tank ranging
        from 2 to 20 feet in diameter, it stretches to match the tank
        diameter.  The digital readout display temperature changes to
        0.001 degrees Fahrenheit.  It can monitor up to four tanks
        simultaneously.  Currently, the above temperature measurement
        system is used instead of the system with "stoddard solvent,"
        which was used in the past.

     •  Water Table—When a high water table is suspected, a standpipe
        device can provide the necessary head pressure to prevent the
        masking effect.  In this situation, the volume change is
        measured in the standpipe.

     •  Tank Deformation—If it is necessary to stabilize tank end de-
        flections, a standpipe device can provide the necessary head
        pressure to eliminate this effect.  Also, if the tank is filled
        up into the fill pipe the night before or at least four hours
        prior to the test, this will allow tank ends to stabilize.

     •  Vapor Pockets—When it is necessary to stabilize entrapped vapor
        pockets, a standpipe device can provide the necessary head
        pressure to reduce vapor pocket effect.  Vapor pocket volume is
        reduced by pressurization of the standpipe with regulated
        pressure.
                                   69

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   To eliminate the vapor pocket effect after a tank is filled up,
   if the standpipe device is not used, the vapor pockets are
   released by a "float tube" device designed for this purpose.
   The opening of the tube is connected to a float.  Therefore, it
   is always situated at the top of the product in a tank (20).

•  Evaporation—Since the test is usually conducted overnight, not
   in the heat of the day, evaporation effect is reduced especially
   when a test is conducted with the standpipe (20).

•  Piping Leaks—If a leak is detected by EZY-CHEK tank testing,
   the EZY-CHEK line testor is used to detect the leak in the
   lines.

•  Wind—If the weather is windy, the vent pipe is covered with a
   cap (20).

•  Vibration—To minimize vibration effects, vehicles with con-
   siderable vibration effects are not allowed in the testing area
   or a test is conducted with standpipe (20).

•  Noise—The effect of this variable on testing accuracy is
   insignificant (20).

•  Equipment Accuracy—The recorder can easily detect a change of
   0.005 inches in the liquid level.  The temperature readout could
   be performed with 0.001 degrees Fahrenheit accuracy (5,18).

•  Operator Error—This will be minimized by training and careful
   consideration of testing procedure (20).

•  Type of Product—Testing could be performed with any type of
   product as long as air could be bubbled through the product and
   evaporation effect is insignificant (20).

•  Power Variation—Recorder motor is spring wound and no
   electricity required.  The temperature monitoring system is
   supplied with a 12-volt battery pack.

•  Instrumentation Limitation—The detection method can be used for
   any type of liquid petroleum fuel storage tank (20).

•  Atmospheric Pressure—The same barometric pressure is exerted on
   the liquid and the recorder's bellows; therefore, this variable
   does not affect test results (5,18).

•  Tank Inclination—This effect is eliminated by recorder cali-
   bration by known volume at the beginning of a test (5,18).
                              70

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     Engineering Comments—In the EZY-CHEK testing method, the Leak
detection accuracy may be affected due to the following reasons:

     •  Difference between measured temperature change and the actual
        temperature change in the tank during a test period.

     •  Leak rate reduction due to the water table level.

     •  Unidentified vapor pockets.  This is because the efficiency of
        the float tube has not been experimented thoroughly enough to
        assure that it could release all the existing vapor pockets in a
        tank.

     •  Product evaporation, when testing is performed on hot nights.

     •  Occurrence of wave due to wind and vibration.  However, this
        effect is partially corrected by the chart results evaluation.

     •  Difference of theoretical tank volume and actual tank volume.

     •  Effect of atmospheric pressure change on vapor pocket volume (if
        any).

6- Fluid-Static (Standpipe) Testing (7,9,10,11)—

     Description of Method (9,10)*—This detection method is known as
"Hydrostatic Testing."However, hydrostatic terms refer to testing with
water, but in underground tank testing the test is conducted with the
product in the tank which is being tested.  Therefore, in this text,
"fluid-static" is used as a correct term for hydrostatic testing.

     A standpipe is filled to pressurize a completely filled tank.  The
pumps in the siphon systems are removed from service and the manifold
vent lines are disconnected.  The pressure exerted by the fluid in the
standpipe is generally enough to provide five psi pressure at the bottom
of the tank. The volume change is calculated from the level change in
the standpipe.

     This method is not a manufactured system and can be used without
special training by the gasoline service station operators.  However,
the method is not adequate for detecting slow leaks nor for determining
tank system tightness and has an unspecified accuracy.  Because the
volume change due to a leak is accumulative, the accuracy of the test
will increase if a long testing period is used and the system is near
temperature and mechanical equilibrium.
*Reported
                                   71

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     Techniques to Compensate for Effects of Variables—This method does
not compensate for the volume changes due to temperature changes, tank
deformation, vapor pockets, and for evaporation for testing.  However,
when the testing time is increased, the effects of tank end deflection
and other variables could be reduced in the final testing result.

     Special precaution should be taken so that pumps in the siphon
systems are taken out of service and that manifold vent lines are
disconnected.

     Engineering Comments—Due to the lack of compensation for major
variables which affect the testing accuracy (unless a long testing
period is used) this method is not adequate as a precision testing
method to detect small leaks.  An apparent loss of product is observed
due to the expansion of the tank volume from tank end deflection and
temperature changes.  The magnitude of this apparent loss can be sub-
stantial.  To detect a leak in this system, the leak must be greater
than the volume variation resulting from tank end deflection and
temperature changes.  These effects could be minimized by using a long
time period and permitting deflection equilibrium conditions.

     The standpipe test method does not require specialized equipment or
personnel.  The testing is time consuming and the accuracy is unspeci-
fied. However, fluid-static testing is more sensitive than the pneumatic
testing (9).

7- Heath Petro Tite Tank and Line Testing (Kent-Moore Testing)
(4,5,7,9,10,11)—

     Manufacturer's Description of Method (4)—This test is essentially
a fluid-static (standpipe) test.  The tank and standpipe (installed in
the tank opening) are completely filled.  A loss can be observed and
measured to 0.01 gallons.  A one-gallon graduate is used to measure the
exact amount of gasoline added to or drained from the standpipe to main-
tain a constant level.  The constant level results in a uniform tank
pressure.

     A circulating pump draws gasoline from at least six inches below
the tank top through a suction tube; if necessary, the tube is
lengthened by a hose extension.  The gasoline is discharged under
approximately 25 pounds per square inch pressure through a discharge
hose into sections of tubing which have been coupled together to form an
outlet jet at the bottom of the tank.  This jet is adjusted to be above
any water in the tank bottom and is adjusted to be below any drop
tube.  The jet is directed 45 degrees upward from the center line of the
long tank axis.  These suction and jet systems create a vortex-like
swirling motion in the tank and attempt to produce a uniform temperature
throughout the tank.  Figure 18 illustrates the Petro-Tite testing
method.
                                   72

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                   GRADUATED CONTAINER
                                STAND PIPE
                         AIR SEAL-*

                      THERMISTOR
              DISCHARGE NOZZLE-
                                      PUMP
                                 INLET
                         /            V-
THERMAL SENSOR
S.
     PIPE   110V 1 PHASE
                                          STORAGE TANK
           Figure  18.  Petro Tite  Installation (4)

Ref:   Heath Consultants  Inc., Petro Tite Tank Tester Bulletin
                              73

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     The uniform temperature obtained by circulation is electrically
measured by a thermistor in the bottom of the suction tube.   The
thermistor is located approximately 6 inches below the top of the
tank.  Temperature changes are constantly measured.  Volume  changes are
calculated from the temperature changes.  The calculated volumes are
subtracted from the volume change measured by the graduate.   Measured
volume changes are due to tank end deflection or leakage.  Any dif-
ference between the calculated and measured volumes in the 15 to 30
minutes after tank end deflections cease, (approximately two hours), is
considered to be leakage if it is equal to or more than 0.05 gallons per
hour.

     The minimum time to perform the test is 2.5 hours.  The entire test
can usually be completed in one working day (10).

     Manufacturer's Techniques to Compensate for Effects of  Variables
(4)—In the Petro Tite testing method, the following effects of vari-
ables are compensated as described below:

     •  Temperature—This is done by using a thermal sensor and a
        temperature monitoring system.  During the test, the product is
        constantly circulated to attain an average temperature.
        Circulation time is five to eight minutes per 1,000 gallons;
        five minutes for lighter liquids (gasoline) and eight minutes
        for heavier liquids (fuel oil).  The thermal sensor is attached
        to a semiconductor thermistor probe in the tank and is capable
        of discerning 0.003 degrees Fahrenheit changes.  By passing a
        small electric current through the thermistor, the average
        temperature is measured at the point of withdrawal six inches or
        more below the tank top.  However, due to the overall accuracy
        and repeatability of the thermal system, the exact fraction of a
        degree Fahrenheit (i.e., 0.003 degrees Fahrenheit) varies
        slightly at different temperatures, which may cause some in-
        accuracy in the measurement of actual temperature changes.  A
        chart gives the fraction for any temperature.  Because the test
        takes several hours, accurate temperature monitoring can be
        accomplished.

     •  Water Table—The leak masking effect due to a water table  is
        eliminated by inducing a constant pressure gradient on a leak.
        In addition, in areas with a water table and when there is no
        data available on the water level, the data should be obtained
        by drilling a monitoring well, prior to a test.  The water level
        is used to determine the product level in the standpipe for
        testing.

     •  Tank Deformation—Apparent volume changes are compared with a
        chart to recognize  the occurrence of tank end deflection.
        Volume changes are  observed in equal time  intervals and recorded
        on the Tank Test Data Chart.  The manufacturer  reports
                                    74

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        diminishing  apparent  losses  in equal  time  intervals  as  end
        deflection occurs.

        A technique  has  been  developed to  quickly  eliminate  these
        apparent  losses  due to  tank  end deflection.   A high  level, and
        therefore a  greater pressure,  is maintained  at the beginning of
        the  test  in  the  standpipe.   When recorded  data indicate steadily
        decreasing losses,  the  product level,  and  therefore  the pres-
        sure,  is  lowered,  and tank end deflection  usually disappears
        within two hours.

     •  Vapor  Pockets—The  presence  of vapor  pockets in the  tank is
        recognized by  direct  observation of the bubbles in the  stand-
        pipe.   This  is due  to product  circulation  for temperature
        monitoring which carries  some  of the  air to  the fill pipe.

     •  Evaporation—Product  loss by evaporation is  minimized by using a
        cap  to cover the graduate's  top.

     •  Piping Leaks—For storage systems  with submerged pumping,
        separate  tests must be  run on  the  tank and piping by the tank
        tester and line  tester  units.   On  suction  delivery tank systems,
        the  test  checks  the entire system  simultaneously.

     •  Equipment Accuracy—The product volume change in the standpipe
        (tank) can be  measured  by using a  one-gallon graduated
        cylinder. Volumes  less than 0.01  gallons  can be read on this
        cylinder  (21).  The temperature changes are  constantly  measured
        with 0.003 degrees  Fahrenheit  accuracy.

     •  Operator  Error—This  is minimized  by  using a skilled technician.

     •  Type of Product—As long as  the product is of low enough
        viscosity to be  free  flowing,  the  method can be used to detect
        small  leaks  (21).

     •  Tank geometry, wind,  vibration, noise, power variation, and
        instrumentation  limitation do  not  appear to  have significant
        effects on  the applicability and accuracy  of the detection
        method.

     Engineering  Comments—In the Petro-Tite  method, the testing
accuracy to  measure  leak rate may be affected due  to the following
reasons:

     •  Difference  of  measured temperature change  with the actual
        temperature  change in the tank.

     •  Water table  level changing  the leak rate.
                                   75

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     •  Leak rate measurement higher than the leak rate of normal tank
        operations.   This is due to the use of fluid-static head greater
        than normal  operating conditions.

     •  Unidentified vapor pockets.

     •  Difference between the theoretical tank volume and actual tank
        volume.

     •  Effects of atmospheric pressure change on vapor pockets volume
        (if any).

8- Helium Differential Pressure Testing (22)—

     Manufacturer's  Description of Method (22)—This test is an inert
gas pressure test and is used to determine whether an underground tank
is leaking and, if so, at what rate.

     The tank is pressurized with helium after capping off all product
and closing all vent lines connected to the tank.  The tank pressure is
compared to the pressure of a reference probe inserted in the tank.  The
tank pressure, differential pressure, and ambient temperature are
measured at half-hour intervals for a minimum of 48 hours.  The data
provided by these measurements are sufficient to calculate whether any
observed changes in tank pressure are due to leakage from the tank or
are caused by the diurnal variation in ambient temperature.  A leak rate
less than 0.05 gallons per hour can be detected by this procedure.  The
equivalent volume of product lost during the test is computed from
Bernoulli's equation for flow through an orifice.

     Manufacturer's Techniques to Compensate for Effects of Variables
(22)
—In this testing method, the following effects of variables are compen-
sated as described below:

     •  Temperature—The pressure change due to the temperature change
        is compensated by using a reference tube inserted in the tank.

     •  Tank Deformation—The effect of tank end deflections is reduced
        by the 48-hour testing period (23).

     •  Type of Product—The type of product stored in the tank is
        compensated by including the product molecular weight in
        computation of gas density.  Computed gas density is used  in the
        leak rate computation.

     •  Vapor  pockets, evaporation, tank geometry, wind, vibration,
        noise, power variation, instrumentation limitation, atmospheric
        pressure, and tank inclination are not applicable in this  method
        of testing  (23).
                                    76

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     Engineering Comments—In this method, testing accuracy may be
affected by the following reasons:

     •  Difference between the compensated (calculated) pressure change
        and the actual pressure change due to the temperature effect.

     •  The masking effect and leak, rate reduction due to a water table
        level cannot be avoided.

     •  Differences between the actual tank geometry and the given
        geometry by tank manufacturer which is used for leak rate
        estimation.

     •  Piping leaks cannot be differentiated from tank leaks.

     •  The error in the measurement of differential pressure is reduced
        by installing the measurement device inside the tank.  In this
        situation, the measurement will not be affected by ambient
        temperature change.

     •  The operator efficiency to tighten and seal the accessible ports
        and flanges.  In addition, operator experience is necessary to
        use the appropriate printed differential pressure result to
        obtain the final leak rate.

9- Leak Lokator LD-2000 Test (Huntef-Formerly Sunmark Leak Detection)
(5,7,10,11,24)--

     Manufacturer's Description of Method (5,24)—This method operates
on the Archimedes Principle of Buoyancy which states, "The apparent loss
in weight of any object submerged in a liquid is equal to the weight of
the displaced volume of the liquid."

     The Leak Lokator consists of a hollow cylinder which is sealed at
the bottom, an analytical balance (weighing scale), electronic
transmitting circuitry, and a strip chart recorder.  A sensor, suspended
from the analytical balance, is placed in the tank liquid.  The weight
of the sensor is equal to its actual weight minus the buoyancy force
from the liquid in the tank.  Any change in liquid level will change the
buoyancy force on the sensor and hence, the weight of the sensor.  The
weight change is monitored by the analytical balance which
electronically transmits a "signal" to the recorder.  The chart recorder
graphically shows volume changes versus time. The angle and length of
the line drawn by the recorder is directly correlated to the quantity
and rate of leakage.  Figure 19 illustrates the Leak Lokator testing
method.
                                   77

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00
              ANALYTICAL  BALANCE
IQUID LEVEL
ENSOR
                                 Figure 19.  -Leak Lokator  Installation (24)

                     Ref:   Hunter Environmental Services, Inc., Leak Lokator LD2000 Bulletin

-------
     The chart recorder notes the lapsed time in minutes versus volume
change in cubic centimeters of the product displaced either into or out
of the tank.  A vertical line shows no change in volume, while lines
with positive or negative slopes indicate decrease and increase,
respectively, in the product volume.  The system is calibrated at least
six times during each test.  This is performed by quickly adding or
removing a calibration rod of precise known volume to the test system.

     Typically, the time for equipment set up and temperature adjustment
is 1.5 hours.  A complete testing on one tank can usually be performed
in 3 to 4 hours, and on four tanks in 8 to 10 hours.  After the
equipment is set up, the test to determine a volume change typically
takes less than one hour.  This time will increase to at least two hours
for in-tank testing.  The least sensitivity occurs when the product
level is near the center line of the tank.  However, even at this level,
volume changes of 0.05 gallons per hour can be detected by adjusting
test time and the electronic signal. The greatest sensitivity for
detecting a small leak is achieved if the testing is conducted with the
liquid in a riser above grade.

     Manufacturer's Techniques to Compensate for Effects of Variables
(5,24)—In the Leak Lokator testing method, the following effects of
variables are compensated as described below:

     •  Temperature—This test compensates for temperature variation by
        lowering a thermistor to the center (midvolume) of the tank and
        measuring temperature change continuously during the test.  The
        product temperature is stratified at various levels throughout
        the tank; however, it has been researched and proven to the
        satisfaction of this manufacturer that the midvolume location is
        a proper location to measure the average rate of temperature
        change for the entire volume as long as the strata are undis-
        turbed, and the tank is buried and not subjected to ambient or
        unusual external effects.  If a tank system is uncovered for any
        reason and subjected to ambient temperatures, or if the system
        is subjected to some other external source of temperature
        change, testing is conducted using three probes equally volume-
        spaced, and the average rate of temperature change is the
        volumetric average of the three probes.  The signal from the
        probe(s) is electronically transmitted to a strip chart recorder
        and displayed on a digital meter with a resolution of 0.001
        degrees Fahrenheit.  The x-axis full-scale strip chart is
        typically set at one degree Fahrenheit (0.01 degrees Fahrenheit
        per division).

        In addition, to enhance the accuracy of the temperature compen-
        sation technique, a precise measurement of the product API
        specific gravity is made, on site, by taking a sample of the
        liquid being tested.  The API gravity and observed temperature
        are then related to the coefficient of volumetric expansion
        using ASTM data.
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Water Table—If the water table level is known, the proper
product level is used to overcome the forces of water outside
the tank.  When the water level is unknown, the test level is
set assuming the water table is above the tank top.  In addi-
tion, the level changes due to temperature changes during a test
period virtually prevent the condition for a leak to be
masked.  This is due to the differences between the forces
inside and outside a tank whenever the level changes.

Tank Deformation—In this method of testing, because the pres-
sure exerted by a fully charged system is only about one pound
per square inch, the tank end deflection is minimized.  In addi-
tion, because the most significant effect of deflection occurs
almost immediately after a system is topped off, end deflection
is typically not a problem.  If for some reason fill pipe
product levels must be raised higher than normal for testing,
charts are provided by the manufacturer to compensate for
related volume changes.  If tank end deflection is significant,
the test slope will be erratic and inconsistent, thereby indi-
cating the need to compensate by raising and lowering the level.

Vapor Pockets—Due to the short duration of the test, vapor
pockets compensation is rarely required because vapor pockets
only affect test results when ambient barometric pressure or
temperature changes significantly during a test period.  If the
pocket size is four gallons or less, and if the barometric
pressure change is less than 0.02 inches Hg per hour, no cor-
rections are needed.  Tables are provided to compensate for
changes greater than 0.02 inches Hg per hour.  In addition, if
vapor pockets are present and affected by temperature or pres-
sure, the test slope will be erratic and inconsistent, thereby
indicating the need to compensate and/or eliminate the pockets
until conclusive results can be obtained.

Product Evaporation—In this method, a hollow sensor is used to
compensate for product evaporation.  This sensor is sealed at
the bottom, filled with the product, and suspended for testing
to a point a few inches higher than the product level in the
tank. The inside diameter at the top of the sensor is slightly
larger than where the sensor enters the product so that the
surface area inside the tube is the same as the surface area
occupied by the tube in the product.  For this reason, evapora-
tion takes place from the surface area of the sensor at the same
rate as from the surface area of the product measured.  As
evaporation occurs from the hollow tube, the sensor becomes
lighter.  However, the buoyancy force exerted on the sensor by
the product in the tank decreases at the same rate due to
evaporation, thus entirely compensating for evaporation effects.
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    •  Piping Leaks—If a leak is found during the full  system  test,
       with the product level raised  so that all buried  piping  is  being
       tested, the level is then lowered to tank top  (within one to  six
       inches) and another test is conducted to check leaks in  only  the
       tank.

    •  Vibration—Vibration factors,  such as traffic  may cause  the leak
       rate slope to fluctuate; however, the rate of  change is  easily
       determined by drawing a slope  through the fluctuations.  The
       most significant effects of vibration occur during in-tank
       testing.

    •  Equipment Accuracy—The reading accuracy for volume change  is
       calculated by chart calibration with addition  or  removal of
       product to optimize the chart  deflection per calibration.   The
       electronic voltage signal is also optimized to minimize  the
       volume calibration per division.  The temperature readout is
       provided at 0.001 degrees Fahrenheit accuracy  on  a digital
       display.  Both  temperature and volume change are  continuously
       recorded.

    •  Operator Error—The operator error is minimized by using a  crew
       of  trained operators (25).  All testing services  are provided by
       Hunter employees.

    •  Type of Product—The method can be performed effectively on any
       products or mixture of products where the sensor  can be  freely
       suspended.

    •  Instrumentation Limitation—The test can be conducted in any
       size underground tank  system with two-inch or  larger opening.
       However, for  in-tank testing,  a minimum opening of four  inches
       is  required.

    •  Atmospheric Pressure—It has been determined that a barometric
       pressure increase during the test period would have to exceed
       0.07  inches Hg  in one  hour  to  effect an apparent  leak of 0.01
       gallons per .hour.  Because  a pressure increase is generally
       slower than a pressure decrease and  therefore  would not  occur
       during the  short test  period,  it  is  normally not  necessary  to
       compensate; however, charts are provided  in the operator's
       manual if  this  unusual circumstance  occurs.

    •  Tank  Inclination—The  effect of tank inclination  is eliminated
       by  testing  calibrations  (25).

    Engineering Comments—In  the Leak Lokator testing, the accuracy  may
be affected due to  the  following reasons:
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     •  Difference between measured apparent  temperature change and
        actual  temperature change.

     •  Leak rate change  due to  the water table effect;  therefore,  the
        water table masking effect  cannot be  avoided.

     •  Tank end deflection, if  it  is  unidentified.

     •  Vapor pockets.  When the volume of the vapor pocket is unidenti-
        fied, there is  no way to measure its  volume  changes due to
        temperature and barometric  pressure changes  during a test
        period.

     •  Occurrence of wave due to wind and vibration.   However, this
        effect  is partially corrected  by the  chart results evaluation.

     •  Difference between theoretical tank volume and actual tank
        volume.

     •  Power variations  due to  the use of 110V AC power source.

     •  In some cases,  the fill  pipe is at such an angle from vertical
        that the sensor could not be installed in the tank without
        touching the wall.  Therefore, tank testing  is not possible by
        this method.

10- Mooney Tank Test Detector (5,7,10,26)—

     Manufacturer's Description of  Method (5,26)—In this method, an
underground storage tank  is filled  with product into the fill pipe.  The
test starts 12 to 14 hours after product delivery.  The product level
and the temperature of  the liquid within the tank are monitored over a
one-hour period with 20-minute testing intervals. A leak as small  as
0.02 gallons per hour can be detected (27).  If the  elevation of the
liquid in the fill pipe changes from the level caused by expansion or
contraction due to temperature changes, and by evaporation loss, this
indicates a leak in the tank.

     In the past, level changes were monitored by either a mechanical
float device or an electronic capacitance probe (27).  The electronic
type could provide a digital readout of 0.01 inches  of level change.  At
the present time, a dip stick graduated at 0.05-inch divisions is used
to measure the level.  One  side of  the dip stick is  covered with gaso-
line or water indicator paste and inserted into a tank.  To increase the
level measurement accuracy, the dip stick is connected to a leveling
device which sits on the opening of the fill pipe.  The instrument box
is capable of testing three tanks at the same time.

     Manufacturer's Techniques to Compensate for Effects of Variables
(5,26)—In the Mooney Leak  Detection testing method, the following
effects of variables are compensated as described below:
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     •   Temperature—The  average  temperature of  the tank is measured by
        monitoring the  temperature  at  the center of each of five Layers
        with  equal volumes.   The  device includes an electronic tempera-
        ture  differential measuring system consisting of five electronic
        sensors  and  digital  readout.   The anticipated accuracy for
        temperature  measurement  is  in  a range of 0.001 to 0.006 degrees
        Fahrenheit.

     •   Tank  Deformation—In this method, the significance of the tank
        end deflection  effect is  minimized by filling the tank up into
        the fill pipe  12  to  14 hours before the  test period.

     •   Evaporation—This system  uses  an evaporation cup as a measuring
        device.   The cup  is  filled  and installed in the fill pipe.  The
        height  of product which  evaporates from  the cup during the test
        period  is measured.   This height is equal to the height of the
        liquid  evaporated from the  fill pipe and will be considered as
        the final resultant  evaporation.

     •   Piping  Leaks—If  a leak  is  detected, the level of the product is
        lowered in the  fill  pipe  to below the top of the tank, and a
        complete set of testing  is  performed (27).   This test will
        identify if  a  leak is in  the piping.

     •   Equipment Accuracy—The  level  measurement device "dip stick" is
        divided to 0.05-inch divisions.  The temperature readout could
        be provided  with  0.001 degrees Fahrenheit accuracy on a digital
        display.

     •   Type  of Product—The type of the product will not affect the
        testing accuracy  as  long  as the level change of liquid can be
        determined on  the product indicator paste (27).

     •   Tank  Inclination—This effect  is compensated by calibration for
        level reading  at  the beginning of each testing period.

     •   Instrumentation limitation  and power variations have insigni-
        ficant  effects  on the detection method (27).

     Engineering Comments—In the Mooney Tank testing method, the
accuracy of the results may  be affected due to the following reasons:

     •   Difference between the measured temperature change and the
        actual  temperature change during the test period.

     •   Leak  rate changes or masking due to water table effect.

     •   Unidentified vapor pocket(s).
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     •  Difference between theoretical tank volume and actual tank
        volume.

     •  Error in level reading due to vibration by wind and traffic.

     •  Operator accuracy in reading the product level changes from the
        dip stick.

     •  Rapid change in barometric pressure.

11- PACE Leak Tester (28)--

     Manufacturer's Description of Method (28)—In testing with the PACE
Leak Tester a tank is nominally filled, at a product level several
inches below the top of the fill pipe, about 12 hours before testing is
started to allow the temperature to stabilize.  The tank's vent and feed
pipes are sealed except for one which is fitted with a "dip tube."
Measurements of the liquid level in the dip tube are taken during the
course of the testing.

     The system consists of a small-diameter tube (dip tube) as the test
tube, a wooden ruler to measure the product level in the dip tube, three
thermocouples to read product temperature, and a barometer to read atmo-
spheric pressure.  The dip tube is welded into a cap that is then
threaded onto the testing tank's fill pipe in such a way that the dip
tube extends above the fill pipe.  It is possible to gain access to the
stored product through this open-ended pipe.  During the tank testing,
this pipe is the only access point to the product.  The presence of the
void above the product level in the tank converts the dip tube into one
arm of a manometer that measures the difference in pressure between the
gas in the void and the atmosphere outside the tank.  The product levels
within the tube and the tank will both change in response to a leak or
to a temperature change.  The change of the void pressure due to a leak
is magnified in the dip tube.  The recommended procedure is to install
thermocouples at three specific locations at the top, middle, and bottom
of the tank.

     Four consecutive measurements of product level in the dip tube, and
temperature measurements are made at approximately half-hour intervals
spanning a 1.5-hour period.  In addition, the atmospheric pressure  is
measured at the beginning and end of the testing.  The results are ana-
lyzed and leak rates are derived using a simplified calculation.

     The computed  leak rates can also be assessed statistically.  The
statistical analysis performed can also be  calculated on the three
estimated leak rates to produce an overall  average and corresponding
standard error.   If  this overall average is not greater than the  largest
of the  four  leak  volume error values,  then  the  experiment  indicates that
a  leak  (if present)  is less  than  the  intrinsic  error  of the  experi-
ment.   If the overall average is  greater than the largest  error,  but  is
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not more than eight ounces per hour greater than the largest error, then
the experiment has not detected a Leak greater than the NFPA leak
detection limit of eight ounces per hour (0.05 gallons per hour).

     The PACE Tank Testing is in principle a simple, accurate, and
practical test, which has been theoretically and experimentally tested
in a program conducted for the Petroleum Association for Conservation of
the Canadian Environment.  This method is not commercially available.

     Manufacturer's Techniques to Compensate for Effects of Variables
(28)—In testing with the PACE Tank Tester, the following effects of
variables are compensated as described below:

     •  Temperature—When a tank is filled with product, the test will
        be conducted after a 12-hour temperature stabilization period.
        Based on statistical evaluation, it is found that three thermo-
        couples are satisfactory to measure the product temperature at
        the top, middle, and bottom of the testing tank.  The accuracy
        of each thermocouple is 0.01 degrees Fahrenheit.  After the
        initial temperature measurements, the measurements will be
        repeated at three equal intervals of a half-hour.  These
        measurements are used to compute the mean value of the expansion
        effect and its standard error.  In some experiments (during the
        summer) this statistical error is the factor limiting the
        accuracy of the measured leak rate.

        The measurements for three test repetitions also allow for a
        statistical estimate of the overall error in measuring the leak
        rate.

        The thermal expansion of the liquid gasoline is the largest
        perturbation in this method and is always significant.  It is
        imperative that thermal expansion be compensated.

     •  Tank Deformation—The fill/empty cycles during the normal oper-
        ation of a tank should compact the backfill material adjacent to
        the tank ends.  This results in a void between the ends and the
        limit of the deflections.  If the movement of the ends is unres-
        trained, the deflection will occur immediately after filling.
        In addition, a 12-hour temperature stabilization period also
        ensures that/ the end deflection is not a significant factor.

     •  Product Evaporation—It is calculated that the effect of product
        evaporation due to the increase of the void volume by a small
        leak is negligible.

        The evaporation effect due to change of product vapor pressure
        by temperature change is compensated by obtaining the vapor
        pressure from the Reid Chart and is based on the top thermo-
        couple temperature reading.
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    •  Tank Geometry—The effect of the tank geometry on the void
       volume above the product level is minimized by initial cali-
       bration.  The initial depth of the product from the top of the
       dip tube is measured with a ruler.  Finally, a measured volume
       of product, about 0.05 gallons, is removed from the tank with a
       syringe inserted into the dip tube.  This creates an artificial
       leak and the new depth of the product in the dip tube is
       measured.  Since these all take place within about one minute,
       the temperature and atmospheric pressure are considered constant
       and hence the artificial leak without expansion effect is
       measured.

    •  Vibration—In this method, due to the magnification of the
       product level change in the dip tube, the vibrations due to such
       things as vehicle traffic do not have a significant impact on
       the results.

    •  Equipment Accuracy—The accuracy of this method is especially
       affected due to temperature variation.  In a 5,000-imperial-
       gallon tank, the intrinsic error in the temperature measurement
       (0.005 degrees Fahrenheit) corresponds to an expansion effect of
       2.5 ounces (0.015 gallons).  The accuracy is increased during
       the winter period.  It is estimated that in this method
       accuracies of 0.125 inches, 0.01 degrees Fahrenheit, and 0.1
       inches of mercury for ruler, thermocouples, and barometer,
       respectively, are sufficient.

    •  Operator Error—This method is invented to provide a method with
       little or no requirement for operator training.

    •  Instrumentation Limitation—Since  the temperature is only
       measureable to the nearest 0.01 degrees Fahrenheit, this
       limitation may be more important than the statistical error
       value.

    •  Atmospheric Pressure—The main effect of a change in atmospheric
       pressure is on the level in the dip  tube.  Other effects  such as
       a change in volume of the tank and the liquid within it are
       bound  to be negligible for  the small changes of pressure  ex-
       perienced  as the weather changes.  In addition, the steel  tank
       and  its  product  contents are  effectively  incompressible.   The
       atmospheric pressure  could  be measured with a barometer at an
       accuracy of 0.1  inches of mercury.   However, under normal
       conditions  the change in atmospheric pressure over the  short
       period of  the  test  (1.5 hours) will  not  significantly affect  the
       results  and hence  this measurement can normally be eliminated.

     Engineering Comments—If the void  space above  the product  level
behaves as an ideal  gas,  the  testing  results with the PACE Tank Tester
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will be theoretically acceptable.  However, any deviation of the void
space from ideal gas behavior will affect the accuracy of the testing.
This method is a developing method with limited experimental trials on
steel underground storage tanks and none on fiberglass tanks.  There-
fore, there is not sufficient data and evidence available to conclude
that the void space behaves as an ideal gas.

     In this testing method, the detection accuracy may be affected due
to the following reasons:

     •  Lack of proper technique to measure the representative
        temperature of the product and the void space.  These will
        affect compensation for evaporation due to inadequate
        estimations of product vapor pressure.

     •  Water table effect on the leak rate cannot be prevented.  In
        some cases, the leak may be completely masked due to the water
        table effect.

     •  Vapor pocket effect may be insignificant, due to short period of
        testing.

     •  Product evaporation due to the dip tube with an end open to the
        atmosphere.

     •  Piping leaks into the tank.

     •  Wind effect on product evaporation rate due to the presence of
        the dip tube with an open end to the atmosphere.

     •  Noise will not affect the detection accuracy.

     •  Type of product will affect the vapor pressure and the rate of
        the evaporation.

     •  The power variation effect can be minimized by using a new
        battery for each tank testing, since the digital thermocouples
        in this method are the only electrical components.

     •  Since the product level is measured in a dip tube with 1.5-inch-
        diameter, the tank inclination effect on the detection accuracy
        will be insignificant.

     •  The precision of the method is overstated (the entire
        statistical analysis should be carefully reviewed).

12- PALD-2 Leak Detector (10,29)--

     Manufacturer's Description of Method (29)—In this method, a
completely filled underground storage tank is pressurized with nitrogen
to allow the level to rise within a sensing column to a viewing window
above ground level.  The tank is pressurized to at least three different
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pressures during the course of testing.  All ports and vents to the
atmosphere must be closed and/or sealed.

     The system consists of a nitrogen cylinder, a pressure measuring
device, a series of electro-optical level sensors, a microprocessor, and
a printer.  The level changes are detected through electro-optical
sensors.  The microprocessor determines the validity of the readings and
sends the calculated leak rate to the printer.  The leak rate is cal-
culated based on the size of the leak and on the pressure difference
across the leak.  The testing depends on the requirement to rapidly
settle the tank after each pressure change.  This is accomplished by
raising the gas pressure above the test pressure for a short duration.
Care must be taken not to go beyond the equilibrium point.  The
sensitivity of the system is high (less than 0.05 gallons per hour) and
monitoring time short (less than 15 minutes).

     Manufacturer's Techniques to Compensate for Effects of Variables
(29)
—In the PALD-2 testing method, the following effects of variables are
compensated as described below:

     •  Temperature—The temperature effect is minimized by the short
        duration of the testing in an equalized condition.

     •  Tank Deformation—The effect due to this variable is minimized
        by the short duration of the testing in an equalized condition.

     •  Vapor Pockets—Presence of entrapped air has a serious negative
        effect on the test quality and it should be removed prior to
        testing, at all cost.

     •  Instrumentation Limitation—Care must be taken not to go beyond
        the equilibrium point.  If this occurs, the tank will contract
        during the measurement and a negative volume change will be
        indicated.  In this case, the test may be abandoned and repeated
        at a later time or the microprocessor may be reprogrammed to
        repeat the test at a slightly higher pressure.

     •  Other sources of error are:  ground water table, ground motion
        introduced by external sources, oscillations within the tank
        system, and atmospheric pressure changes.  However, the method
        to reduce most of these errors is to allow ample time for the
        tank to settle.

     Engineering Comments—In this testing method, the detection
accuracy may be affected due to the following reasons:

     •  Temperature effect on volume change may be significant, as  com-
        pared to the measured volume change during a short testing
        period.
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      •   Leak rate change by the water table effect and leak rate
         enhancement  due to the application of pressure greater than the
         normal  operating condition.

      •   Piping  leaks.

      •   Equipment accuracy.

      t   Power variations.

      •   Product evaporation,  tank geometry, wind,  operator accuracy,
         type of product (with similar vapor pressure), and tank
         inclination  do not appear to affect the quality of the test.

      In addition, in this testing method,  the following disadvantages
 are noticeable:

      •   Due to  the use of pressure greater than the normal operating
         pressure, the leak rate increases  during the course of testing.

      •   There is a risk that  tanks weakened by corrosion will be
         ruptured by pressurization.

 13- Pneumatic Testing (7,9,10,11)—

      Description of  Method (9,10)*—In this method, which is not a manu-
 factured system, the storage  tank and the  piping systems are pressurized
 with air or another  gas.  The pressure change depends on the change of
 gas volume in the tank and piping.  However, this  method does not com-
 pensate for any variable changes during the testing period.  The method
 is not  sensitive to small leaks and is not likely to detect leaks below
 the liquid level in the tank.  In addition, the piping and tank leaks
 could not be differentiated from each other.

      Techniques to Compensate for Effects  of Variables (9,10)*—The tank
 end deflection effect could be reduced during the  testing period.  How-
 ever, this method will not compensate for  other variables which may
 affect  the testing results.  Greater accuracy can be achieved, when the
 tank is full or nearly full.

      Engineering Comments—In the pneumatic testing method, the follow-
 ing problems could be noticed:

      •  Air pressure and vapor pressure of the stored liquid in the tank
         vary greatly with temperature.  The temperature effect can be
         measured, but this method does not compensate for pressure
         changes resulting from temperature variation and tank end
         deflections.
*Reported
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     •   Water  table  changes  in  or  masking  of  the  leak  rate  cannot  be
        avoided.

     •   The  method does  not  compensate  for pressure  changes due  to tank
        end  deflections.

     •   If the pressure  exceeds the  tank's normal operating pressure,
        there  is  a risk  of  tank rupture, especially  if the  tank  is badly
        corroded.  The more  product  in  the tank,  the more the  risk of
        overpressurization  should  be considered.

     •   A faulty  or  inaccurate  gage  may allow overpressurization and
        lead to a tank explosion or  rupture.   This should not  happen  if
        equipment is properly calibrated.

     •   Potential increase  in leak rate during the test period (and,
        possibly, after).

     •   Testing with air in tanks  containing  flammable and/or  com-
        bustible  liquids is  extremely hazardous (3).

     •   Due  to the exertion of  additional  pressure on  the tested tank,
        product may  be  forced out  of the tank at  leaks during  the test
        period.

     •   The  method  is time  consuming and the  accuracy  is unspecified.

14- Tank Auditor  (30)—

     Manufacturer's  Description of Method  (30)—This is an  electro-
mechanical  system for detecting leaks in underground piping and tank
systems.  The  method operates on the Archimedes Principle of Buoyancy,

     The major component of this system consists  of a  product  height
deviation transducer, a temperature  probe  height  deviation  transducer, a
temperature  probe,  and a recorder.  A force deflection transducer sup-
ports a negatively  buoyant  member  within the  liquid-filled  fill pipe.
Buoyancy forces are  changed due to product level  change and create a
linear deflection of the force  transducer that is sensed by a noncontact
electronic probe with a voltage output  proportionate to the deflection
of the force transducer.  The temperature probe,  consisting of a thin-
walled hollow cylinder closed at the bottom and opened at  the top, is
placed into the fill pipe.   The length of this probe is equal to or
greater than the tank diameter.  The probe is filled with product.  A
force transducer, similar to the product height deviation transducer,  is
used to sense height deviations within the probe.  A recorder receives
the output voltage  from the transducers and the results are printed on a
strip chart.  At the end of a  15-minute test, the recording is
stopped.  The total volume change due to a leak  is calculated.  At the
beginning and end of each test, both transducers are calibrated by
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addition and/or removal of known volumes of the product from the
temperature probe and the tank.

     If the tank is filled prior to a test, the test is conducted at
least three to four hours after tank fillup (31).  The average time
required to test a single tank, including setup and dismantling, is one
hour.  Typically, an additional hour of testing is required due to
unusual situations such as piping leaks, tank leaks, presence of an air
pocket, syphon systems, and common vents.  The detection method has an
accuracy of 0.05 milliliters (0.00001 gallons) gross volume change in a
four-inch fill pipe and 129 milliliters (0.03 gallons) gross volume
change in a half-full, 10.5-foot-diameter tank.  Therefore, the tank
could be tested even when it is partially full.

     Manufacturer's Techniques to Compensate for the Effects of
Variables (31)—In the tank auditor detection method, the following
variables are compensated as described below:

     •  Temperature—A thin hollow copper tube, filled with product, is
        used for temperature compensation.  This probe can be used when
        the fill pipe diameter is larger than three inches.

     •  Water Table—The complete masking effect of ground water is
        eliminated by performing tests at the bottom and the top of the
        fill pipe.  Because the static head changes, a leak cannot be
        completely masked.

     •  Tank Deformation—If the system is filled prior to a test, major
        tank deflection occurs immediately after tank fillup.  Further
        effects will be reduced or eliminated by three to four hours
        waiting period before a test.

     •  Vapor Pockets—If the presence of vapor pocket is recognized,
        the level of the product will be lowered below the tank top and
        the test performed.  However, piping leaks will not be deter-
        mined and the time for testing will be increased.

     •  Product Evaporation—Because the product level changes due to
        product evaporation in the fill pipe (or fill tube) and in the
        temperature probe are equal, the effect is compensated for
        simultaneously with compensation for temperature change.

     •  Piping Leaks—Piping leaks are determined by performing tests at
        the bottom and the top of the fill pipe.  If a leak is
        identified, the elevation of the leak will be determined by
        adjusting the product level.

     •  Tank Geometry—When the tank is partially filled, this effect is
        eliminated by the testing calibration.
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    •  Wind—Wind effect  is minimized or eliminated by electronic
       dampening and  performing  the  testing under a tent.

    •  Vibration—This method  is  relatively insensitive  to vibration
       due to mounting on the  tank fill pipe.

    •  Equipment Accuracy—A level change due  to 0.05 milliliters
       (0.00001 gallons)  volume  change in a four-inch fill pipe  and 129
       milliliters  (0.03  gallons) volume change in a half-full  10.5-
       foot-diameter  tank can  be  measured by the product deviation
       transducer.  The sensitivity  of the temperature measurement
       probe is to  0.015  degrees  Fahrenheit.

    •  Operator Error—This is minimized by defined testing  procedures
       and operation  by trained  personnel.

    •  Type of Product—The detection method could be used for  any
       product as long as the  probes can sink.

    •  Instrumentation Limitation—The fill pipe must be vertical to
       the extent that a  plumb bob can be hung four inches into  the
       liquid from  the top of  the fill pipe at any point on  the
       circumference  of the pipe without touching the side of the fill
       pipe at the  lower  end.  The probe must  hang vertically into  the
       product from the fill line, vent, or manhole.  Some fill  pipes
       are at such  angles from vertical that testing  is  not  possible.
       A piping and tank  'system  test is always possible.   In addition,
       the temperature probe can be  used when  the fill pipe  diameter  is
       larger than  three  inches.

     •  Tank  Inclination—As long as  tank inclination  does  not prevent
       the equipment  utilization, its  effect  is eliminated by
       calibration  of the chart  at the beginning and  end of  a test.

     •  Noise, power variations,  and  atmospheric pressure do  not
       generally  affect  the detection  method  accuracy.

     Engineering  Comments—In  the Tank Auditor  detecting  method,  testing
accuracy  may  be  affected  by:

     •   Difference between the  product  level  changes  in  the tank and the
        reference  tube due to  temperature  change.

     •   Leak rate  changes  due  to  the  water  table effect  cannot be
        avoided.

     •  Volume changes due to  an  unidentified tank end deflection three
        to four  hours after tank fillup,  during a  testing period.

     •  Unidentified vapor pockets in a completely filled tank.
                                   92

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     •  Power variations.

     •  Effect of atmospheric pressure change on vapor pocket volume (if
        any in a completely filled tank).

15- Two-Tube Laser Interferometer System (9,10,29,32,33)—

     Manufacturer's Description of Method (29)—The Two-Tube Laser
Interferometer System simultaneously measures the difference in the
height of the product in an open tube and a closed tube initially filled
to the same level.  The height changes in the open tube caused by the
principal noise sources that could hide a small leak in a partially
filled gasoline storage tank (e.g., thermally induced volume changes and
evaporation/condensation) are removed (i.e., compensated for) by
subtracting the height changes in the closed tube.

     The major components of the system consist of the laser inter-
ferometer measurement system, two equal length two-inch-diameter tubes
extending to the bottom of the tank, an aluminum float (for each tube)
containing a cube-corner reflector, and a data acquisition system.  The
laser system consists of a laser head, laser display unit, a beam
splitter, and two interferometers mounted on a solid cast aluminum
stand.  The laser head generates a safe, low-power (200 yW) beam which
is divided into two beams for the height measurements in each tube.
Because the interferometer is not attached to the laser head, motion of
the laser head does not' affect the measurement.  The data acquisition
system receives the laser interferometer height measurements made at a
200 Hz sample rate, averages the data over a 42-second period, and
generates a time series at one-minute intervals for the leak detection
analysis.  Figure 20 schematically illustrates the system.

     The laser interferometer measurement system itself measures height
changes to one micro-inch (0.000001 inch).  The accuracy of the Two-Tube
Laser Interferometer System to measure a known product level change is
60 micro-inches? this was determined by making repeated measurements of
the height changes in an 8,000-gallon storage tank produced by inserting
and removing several different solid aluminum bars of known volumes.

     The accuracy of the system for detecting small leaks in an under-
ground storage tank was estimated from the analysis of data collected
during many field experiments (29).  The analysis showed that a leak
rate of 0.041 gallons per hour could be detected with a probability of
detection of 95 percent and a probability of false alarm of 0.1 percent
assuming the tank was 75 percent full.  The time period of the tank test
to achieve this performance is two hours.

     The system was used in an experimental program conducted for the
American Petroleum Institute (29,32,33) and is not available on the com-
mercial market.
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               BEAM SPLITTER
INTERFEROMETER 8
        LASER
       INTERFEROMETER A
              GRODNO
          OPTICAL GLASS-
     GASOLINE SURFACE
                   FLOATS4
           CUBE-CORNER
             REFLECTORS

         GASOLINE
         NEEDLE VALVE
   TWO  BRASS
   TUBES
           Figure 20.  Two-Tube Laser Interferometer (32)

Ref:  Underground Tank Testing Symposium, Petroleum Association for
     Conservation of Canadian Environment (PACE), May 25, 26, 1982
                             94

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     Manufacturer's Techniques to Compensate for Effects of Variables
(34)
—In the Two-Tube Laser Interferometer System testing method, the
following effects of variables are compensated as described below:

     •  Temperature—Because the method uses two tubes (one closed and
        one open end tube), the temperature effect is compensated
        automatically (29,32,33).

     •  Water Table—If the first testing result indicates a nonleaking
        tank, the water table masking effect could be checked by con-
        ducting the test at levels lower or higher than the level in the
        first test (or by measuring the depth of the water table).

     •  Tank Deformation—The effect of this variable is eliminated
        because the test is performed at normal operating conditions.

     •  Vapor Pockets—Vapor pockets are not a problem because the
        testing procedure does not require the tank to be full.

     •  Product Evaporation—Since the level changes due to product
        evaporation in the open and closed (reference) tubes are equal,
        this effect is compensated for simultaneously with the compensa-
        tion for temperature changes.

     •  Tank Geometry—This does not affect the result because the
        system is calibrated for level changes due to a known volume
        change, before the test.

     •  Vibration—Waves in the tank due to the vibration effect is not
        a problem because the raw laser height data is averaged over a
        time period which is long compared to the wave period.  In
        addition, vibration of the ground is not a problem because these
        effects are small and are removed by the two-tube measurement.
        Also, vibration of the laser head is not a problem because the
        laser is separated from the interferometer.

     •  Equipment Accuracy—The resolution of the Two-Tube Laser
        Interferometer measurement systems used in field tests is
        1 micro inch.  The data acquisition system is used to store the
        data after rounding off the data to the nearest 10 micro
        inches.  The system's reported accuracy is within ±60 micro
        inches.  The height change associated with a 0.05-gallons-per-
        hour leak in a 3/4-full, 8,000-gallon, 8-foot-diameter tank is
        530 micro inches.

     •  Type of Product—The type of product will not affect the testing
        accuracy.
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     •  Tank Inclination—The effect due to this variable could be mini-
        mized by calibration of the system on site.

     Other potential sources of error in the height measurement were
investigated:  thermal expansion or contraction of the laser equipment
and mounting stand, thermally induced changes in the tubes' diameter,
vertical alignment of the beam, changes in the refractive index of the
light between the interferometer and the corner-cube reflectors, settle-
ment of the mounting stand, and expansion or contraction of the ground
relative to the gasoline storage tank.  Each of these errors were theor-
etically estimated, quantified experimentally, and rejected because they
were small.

     Engineering Comments—In the Two-Tube Laser Interferometer testing
method, testing accuracy may be affected by the following:

     •  Differences between product level changes in the tank and the
        reference tube due to temperature change.

     •  Leak rate change due to the water table effect cannot be
        avoided.

     •  Vibration, strong enough to produce long waves which masks
        height changes due to a leak.

     •  Operator skill to set up the test equipment.

     •  Power variations.

Nonvolumetric (Qualitative) Leak Testing Methods

1- Acoustical Monitoring System (AMS) (35)—

     Manufacturer's Description of Method (35)—The acoustical monitor-
ing system can be used for detection of leaks in an underground storage
tank.  This system includes the development of advanced instrumentation
for signal detection and processing, the development of signal interpre-
tation methodology, and the use of the triangulation technique for
locating leaks.  Acoustic signals, generated when pressurized liquids
escape through a metal boundary, are detected by piezoelectric trans-
ducers attached to the surface of the pressure boundary.  Nitrogen is
used to pressurize the tank.  In this measurement, accelerometers
(resonant at 27 kHz) are used in conjunction with a wave guide mounted
acoustic emission sensor (resonant at 250 kHz).  With this combination
of sensors, the range of frequencies of flow-induced vibrations and
elastic waves due to a leak can be monitored.

     In an actual field test, the AMS system was able to detect leaks,
as indicated by the Petro-Tite system, of 0.01 gallons per hour.  This
method is not commercially available and is subject to more experimental
studies.
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     Manufacturer's Techniques to Compensatefor Effects of Variables—
The major variables considered for volumetric testing systems are not
applicable to this method.  In addition, other variables are not
identified by the manufacturer which can affect the testing accuracy.

     Engineering Comments—For the AMS detection method, the following
are noted:

     •  Does not provide leak rate.

     •  If the nitrogen pressure exceeds the tank's normal operating
        pressure, there is a risk of tank rupture, especially if the
        tank is badly corroded.

     •  Potential increase in leak rate during the test period (and,
        possibly, after).

     •  The testing method on tanks containing flammable and/or
        combustible liquids is extremely hazardous (3).

     One of the advantages of the AMS method is the capability of
determining the leak's location in the tank.

2- Leybold-Heraeus Helium Detector, Ultratest M2 (5,7,10,36)—

     Manufacturer's Description of Method (5,36)—In this method, helium
is used as a tracer gas for leak detection.  With the vent line plugged,
the tank is pressurized with helium gas to four pounds per square
inch.  The gas is fed at the bottom of the tank so that it mixes
thoroughly with the product in the tank.

     To detect helium, five small holes must be drilled and located over
the corners and center of the tank.  The sniffer probe of the detection
system samples the gas in each hole and the helium is detected using
mass spectrometric techniques.

     Manufacturer's Techniques to Compensate for Effects of Variables
(5,36)—The testing method can detect leaks only by detection of helium
through the monitoring holes outside the tank and is thus not affected
by the variables discussed for other methods.

     Engineering Comments—The method cannot measure leak rate.  In
addition, due  to the presence of product in the tank, ground water, and
ground characteristics (especially for tanks with clay backfill), test-
ing may require a long period of time before a small leak is detected.
One other reason which reduces the detection speed is that helium does
not flow  freely through liquid (37).  However, the method does not
require the tank or pipes to be removed from service during the testing.
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     The five holes may provide an approximation of the location of the
leak (if further tracing of the leak is required).

3- Smith & Denison Helium Test (7,37)--

     Manufacturer's Description of Method (37)—This method of leak
detection is based on differential pressure loss in the tank being
tested relative to a reference steel chamber equipped with a differ-
ential pressure manometer or gage.  Excess pressure (over ambient
pressure) is induced by inserting helium gas into an empty tank and the
reference chamber.  The pressure loss with time is monitored to indicate
leaks in the system.  In addition to pressure loss, gas escaping from a
leaky system is detected, at ground level, by sampling the gas in the
soil pore space and measuring the concentrations of helium by a mass
spectrometer.  This requires drilling small holes into the soil around
the tank or pipe.  Testing is performed in two steps—one step with the
product in the tank (no level change prior to the test) to verify the
tank and piping are sealed above the product level (this test can
usually be performed in less than four hours while the tank is in ser-
vice) and one step when the tank is completely empty.  The pressure
change in the test tank resulting from temperature change during the
test period is compensated for by the pressure change of the reference
chamber.  The reference chamber can be in thermal equilibrium with the
helium gas in the tank one hour after the testing is started (38).
Leaks from tanks usually are detected very quickly.  A search for helium
gas around the tank is conducted soon after differential pressure
equilibration.  In some cases where the tank is protected by a clay
backfill, it may be necessary to continue the test for 24 hours before
helium gas is detected at the soil surface.  If the concentration of the
helium in the soil gas is more than five ppm (helium concentration in
the air), the system is leaking.  In this method, the size of the leak
opening and therefore the maximum possible fuel leak rate could be
calculated.  The manufacturer's literature did not quantify a leak rate
(38) because it depends on the location of the leak in the testing tank,
but did describe the relationship between the size of an opening and the
overall measured helium loss during the testing.

     Manufacturer's Techniques to Compensate for Effects of Variables
(37)
—In this testing method, the following effects of variables are compen-
sated as described below:

     •  Temperature—A reference steel chamber is used to compensate for
        pressure change due to temperature change, which is done by
        measuring  the differential pressure of the tank and the
        reference  chamber during a test period.  The reference chamber
        can be  in  thermal equilibrium with the helium gas in the tank
        one hour after the testing is started (38).
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     •  Water Table—The presence of a high water table surrounding the
        tank prevents the exit of helium from the tank.  However, this
        can be overcome by increasing the helium pressure until it
        exceeds the ambient pressure and can then bubble up through the
        liquid to the surface.

     •  Tank Deformation—This effect will be eliminated by evaluation
        of the printed record on pressure differential of the tank which
        is conducted for at least four hours (38).

     •  Piping Leaks—These leaks could be identified during the first
        step of testing, when the test is conducted with product in the
        tank, and/or during the second test by the detection of high
        concentrations of helium around piping.

     •  Equipment Accuracy—Differential pressure is measured by a
        manometer or an electronic differential pressure gage, installed
        inside the tank, with 0.01 or 0.1 inches of water reading
        accuracy (37).  The sensitivity of the helium leak detection
        method is sufficient to indicate leak size which would result in
        a gasoline leaks as small as 0.005 gallons per hour.  However,
        because the leak rate is dependent on the location of the leak,
        this method cannot provide the actual leak rate (38).  Modern
        helium mass spectrometers can detect helium concentrations as
        Ipw as 0.1 parts per million.

     •  Operator Error—Prior to conducting the test, all the ports are
        sealed by the testing operator.  However, a potential source of
        error is helium leakage through these ports even after they are
        tightened by the operator.  However, this method is capable of
        identifying these types of leaks.

     •  Atmospheric Pressure—The effect of barometric pressure change
        is eliminated by using a device to measure differential
        pressure.

     •  Vapor pockets, product evaporation, tank geometry, wind,
        vibration, noise, type of product, power variation, instrument
        limitation, and tank inclination are not applicable to this
        testing method (38).  One of the disadvantages of this method is
        that helium does not flow freely in a liquid; therefore, the
        tank should be completely empty prior to testing.

     Engineering Comments—In this method, the following points may
affect testing accuracy:

     •  Differential temperature response of the reference chamber to
        actual temperature changes in the tank.

     •  Pressure change due to unidentified tank end deflection.
                                   99

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     •  Leakage due to piping and flanges.

     In addition, this test cannot provide an actual leak rate under
normal conditions, especially when there is a high water table around
the tank.

4- TRC Rapid Leak Detector for Underground Tanks and Pipes (39)—

     Manufacturer's Description of Method (39)—This method, which is
not commercially available, uses volatile and environmentally safe
tracers.  One to three liters of tracer gas are added to the liquid
product.  The tracer compound moves from the leaking tank or pipeline
through any leak.  High-volume pumping in the backfill surrounding the
tank draws the tracer from the leak point to a monitoring pipe where the
soil gas is sampled and subjected to field chromatographic analysis.
The tracer plume is then probed upgradient to locate the leak point.

     This method allows remedial measures to be implemented before
significant environmental damage has occurred.  If more than one system
is suspected, different tracers can be used to test several systems at
once.

     Manufacturer's Techniques to Compensate for Effects of Variables
(39)—The testing method can detect leaks only by detection of the
tracer gas outside a tank.  High-volume pumping is used to speed the
tracer gas transfer to the detection points.

     Engineering Comments—The TRC Rapid Leak Detector cannot measure
leak rate.  In addition, due to the presence of product in the tank,
ground water, and ground physical characteristics (especially for tanks
with clay backfill), the testing may take a long period of time before a
small leak can be detected.  One of the reasons is that the tracer gas
does not flow freely through the liquid (37).  However, the method does
not require the tank or pipes to be removed from service during the
testing.

5- Ultrasonic Leak Detector, Ultrasound (40,41,42,43)—.

     Manufacturer's Description of Method (40)—Utilization of ultra-
sound to detect leakage in underground storage tanks is a possibility.
For the past 15 years, portable ultrasonic sensors have been utilized to
locate pressure and vacuum leakage in a variety of systems such as power
plants and chemical plants.  The detection probes sense ultrasonic
emissions produced by a pressure or vacuum leak.  At present, an ultra-
sound system has not been used for tank leak detection; however, it is a
very promising method.  Following is a description of the expected
system performance.
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     By plugging all gas vents and draining the fluid from the tank, a
vacuum can be produced.  The negative gage pressure will draw air into
the tank from the soils surrounding the tank wall through the leak
site.  The entire tank wall can be scanned in seconds because the
detection head is directionally sensitive and can be rotated to detect
the maximum signal.  Piping leaks can be detected at the same time, and
leaks can be pinpointed within a spread of 15 degrees from the apex of
the transducer.  A leak will be noted through headphones worn by the
operator as well as being registered on a meter.

     The ultrasound detection method requires a compact field unit with
headphones and meter.  In addition, the system is designed to record
test results and the location of a leak.  A relatively simple method of
airborne ultrasonic leak detection from existing commercially available
technology can be adapted to locate in-ground leakage in storage tanks
easily and rapidly.

     Monitoring equipment setup for this system will be very simple.
Once set up, only 20 minutes is required to test a tank.  Also, several
tanks can be tested simultaneously.  The detection system can be
designed with sufficient sensitivity to measure a leak rate of 0.001
gallons per hour or greater of air (44).  A leak of 0.005 inches in
diameter with a pressure differential of five pounds per square inch can
be detected over 30 feet away.  Therefore, the task of detecting a leak
rate lower than 0.05 gallons per hour is straightforward.

     Manufacturer's Techniques to Compensate for Effects of Variables
(40)
—For the Ultrasound System, the following variables are compensated for
as described below:

     •  Water Table—If the water table surrounds the leak hole, it will
        be detected because the the tank chamber will be in a vacuum
        state so that the pressure differential between the tank
        environment and the ingress ing water droplets will cause the
        water droplets to expand and, due to a low surface tension,
        burst.  This burst will produce a detectable ultrasound (between
        20 kHz and 100 kHz).

     •  Piping Leaks—Because the detection head can be rotated to
        detect maximum signal location, piping leaks will be detected.

     •  Noise—Because the detection sensor is mounted in a closed
        system (the tank being tested), background noise in the
        ultrasonic ranges would not affect the results.  In addition,
        the wave length of ultrasound is relatively short; therefore, it
        is easily pinpointed in the presence of ambient, audible sounds.

     •  Equipment Accuracy—Ultrasound can be designed to sense a leak
        at a rate of 0.001 gallons per hour or greater of air (44).  A
                                   101

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        leak of  0.005  inch in diameter with a pressure differential of
        five pounds  per square inch can be detected.

     •  Operator Error—The system will be equipped with a meter to
        register test  results; this will minimize or  eliminate
        inaccuracy due to operator error (44).

     •  Power Variations—This will not affect  system accuracy because
        it  will  be powered by batteries.

     •  Instrumentation Limitation—The system can be capable of detect-
        ing a leak of  greater than or equal to  0.005  inches in diameter
        with a pressure differential of five pounds per square inch at a
        distance of  30 feet from the detector.

     •  Temperature,  tank end deflections, vapor pockets, product
        evaporation,  tank geometry, wind, vibration,  type of product,
        atmospheric  pressure, and tank inclination do not affect testing
        accuracy (44).

     Engineering Comments—For Ultrasonic leak detecting method, the
following are noted:

     •  No  experimental or field testing has been conducted using this
        system for tank testing.  However, the method is a possibility.

     •  It  will  not  provide an exact leak rate.

     •  It  does  not  consider the effect of ground water level on the
        leak rate.

6- VacuTect (Tanknology) (7,10,45)—

     Manufacturer's  Description of Method (45)—The air pressure above
the liquid in the tank is reduced to offset the pressure head of the
liquid in the tank.   As air is drawn into the tank through a leak,
bubble sounds are detected by a hydrophone worn by the operator.
Characteristics  of the sound permit identification of the leak.  The
approximate size of  the leak can be estimated from the characteristics
of the sound.

     After sealing the ports from the atmosphere, this method can
normally be performed in less than one hour and no waiting time is
required before testing.

     Manufacturer's  Techniques to Compensate for Effects of Variables
(46)
—In this testing method, the following effects of variables are compen-
sated for as described below:
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     •  Water Table—When tanks are situated in areas of high water
        table or the soil around the tank is saturated with water,
        bubbles will not form or will persist for only a short time.
        This situation is addressed by auxiliary sensors which detect
        and measure the ingress of water and indicate water level
        changes during the test.

     •  Piping Leaks—In most cases, piping leaks can be identified when
        the product level is lower than the piping and a "hissing" sound
        is detected by hydrophone during the test.

     •  Noise—The system is capable of compensating for background
        noise during a test.  However, potential noise sources should be
        minimized in the test tank area during the test.

     •  Type of Product—As long as gas bubbles can be created in the
        product, the testing method could be used effectively.

     •  Operator Error—The test can determine leaks by a skilled and
        experienced operator, even in the presence of a water table
        around the tank.

     •  Temperature, tank end deflection, vapor pocket, product evapora-
        tion, tank geometry, wind, vibration, power variation,
        atmospheric pressure, and tank inclination should not affect
        test accuracy.

     Engineering Comments—In the VacuTect testing method, the following
points are noticeable:

     •  Operator experience may affect the accuracy of determining a
        leak rate.

     •  When a tank is old or corroded, tank damage or leak enhancement
        due to a vacuum should be considered.

7- Varian Leak Detector (SPY 2000 or 938-41) (5,7,10,47)—

     Manufacturer's Description of Method (5,47)—This method is based
upon the rapid diffusivity of helium gas through a leak, surrounding
soil, and even concrete and asphalt.  An instrument using mass spectro-
metric techniques monitors helium concentration, which is introduced as
a tracer into the tank under 1 pound per square inch pressure.  Normal
equilibrium time is one hour.  If a very small leak is suspected, or if
the tank is surrounded by clay, it is recommended that the helium pres-
sure be raised to five pounds per square inch pressure and allowed to
equilibrate (dwell) overnight.  Helium, due to its small molecular size
and surface tension, flows through a given leak more than 50 times
faster than gasoline.  The method can detect a leak through which a
0.005 gallons per hour of gasoline would leak.
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     The test is accomplished in two subtests.  The first subtest is
conducted when the tank is at its normal level;  this ascertains whether
the tank top, piping, and penetrations are leak free.  The second sub-
test is conducted when the tank is completely empty.

     Under most conditions, the test can be performed by moving the gas
detector probe over the surface above the tank.   If the day is windy or
a shorter than one-hour dwell time is desirable, small holes must be
drilled through the material above the tank at about six-foot intervals
and the probe held in the holes.

     As a check of the entire system, in the second subtest, a sensitive
differential-pressure gage is manifolded to the tank to determine if
there is a pressure loss during the dwell time.   A pressure loss of
about 0.011 pounds per square inch in 24 hours is equivalent to a leak
that would allow a flow of about 0.05 gallons per hour in an average-
sized tank.

     Manufacturer's Techniques to Compensate for Effects of Variables
(5,47)—In this method, the following effects of variables are com-
pensated for as described below:

     •  Temperature—The method is not significantly affected by
        temperature change.

     •  Tank Deformation—The method is not significantly affected by
        end deflection.

     •  Piping Leaks—Testing can accurately determine the location and
        can estimate the depth of the leak before excavation begins.
        Therefore, piping leaks outside the tank can be identified.

     •  Wind—If the day is windy, small holes must be drilled through
        the material above the tank at about six-foot intervals and the
        probe held in the holes.

     •  Equipment Accuracy—The helium detector is capable of measuring
        concentrations as low as one part per million.  Pressure differ-
        ences as low as 0.001 pounds per square inch can be determined.
         •
     •  Vapor pockets, product evaporation, tank geometry, vibration,
        noise, operator error, type of product, power variation, atmos-
        pheric pressure, and tank inclination do not affect testing
        capability (48).

     Engineering Comments—In the Varian Helium testing method, the fol-
lowing are noted:

     •  The  pressure change due to temperature change is not used to
        evaluate the leak rate.
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     •  The masking or Leak rate reduction effects of the water table
        cannot be avoided.

     •  If the surface above the tank is frozen, small holes should be
        dug to detect helium.

     In addition, the system can only provide the maximum leak rate
without consideration of the location of the leak in the tank.

Inventory Monitoring

1- Gage Stick (49)—

     A simple check is to record product depth with a gage stick at the
station's close of business and again at start of day.  The longer this
period, such as weekends or pump repair servicing, the more accurate the
test.  Gage sticks currently in use can be read to the accuracy of 1/8
inch.  Since gage stick readings will fluctuate slightly because of the
angle of the stick when dipped into the tank, the condition of the tank
bottom and product creep, gaging of the stick into smaller increments
would not increase accuracy.  Therefore, the gallonage represented by
1/8 inch is the possible error which will be recorded in the inventory
records whenever tanks are gaged.  This may result in approximately 12
gallons per 1/8 inch measuring range error for a 10,000-gallon tank
(49a).

2- MFP-414 TLG Leak Detector (50)—

     The MFP-414 TLG is basically used as an inventory monitoring sys-
tem.  A sensor head is placed at the bottom of the tank (Figures 21 and
22).  The sensor is connected via a shielded twisted pair of wires to
the Control Unit.  The Control Unit is located in a nonhazardous area
inside the service station office.  The sensor head consists cf three
pressure transducers referenced to the pressure at the top of the tank;
the bottom and middle transducers are used for water detection while the
top and middle transducers are used for product density measurement.
The absolute pressure at the middle transducer and the density measure-
ment are used to calculate the height of the product.

     The electronic Control Unit can be used for monitoring up to six
tanks and can be installed more than 1,000 feet from any given tank.
The manufacturer indicates that the temperature effect is corrected by
density measurement.  Accuracies of ±0.25 percent and sensitivity of 0.1
percent of product height in the measurement of the product height are
claimed.  Also, for the most accurate overall results, for the total
volume of product, it is recommended that each tank be calibrated in
place to account for any deformities in the tank that may have occurred
during installation.
                                   105

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                     SENSOR   ASSEMBLY
STANDARD 3/4"
ELECTRICAL AND
PLASTIC CONDUIT
                                                SERVICE LOOP
STANDARD 4" FILL
TUBE CAP
                                              DIAPHRAGM FOR
                                              MEASUREMENT OF
                                              SPECIFIC GRAVITY
                                               DIAPHRAGM FOR WATER
                                                   DETECTION
                                            DIAPHRAGM FOR BOTTOM
                                            PRESSURE, SPECIFIC
                                            GRAVITY, AND WATER
                                            DETECTION
   Figure  21.  MFP-414 TLG Leak  Detector-Sensor Assembly  (50)

                 Ref:  Transitron  Controls
                              106

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                     TAMK LEVEL GAUGE & LEAK DETECTOR
           BASIC FUNCTIONS

           -MEASURES LEVEL/VOLUME
           -DETECTS LEAKS
           -DETECTS WATER
                                   • IMOTI COMMUNICATION

                                   VI* TlklfNOn* UNO
                                                        DIGIT LED  DISPLAY SHOWS
                                                       SEALED SWITCHES FOR TANK
-LINEARIZES HORIZONTAL TANKS
 (FROM STRAPPING TABLES
 OR EQUATIONS)
-ACCEPTS  UP TO SIX(6) TANK
 SIGNALS
-ACCEPTS  UP TO SIX OTHER
 SIGNALS
 (FLOW DATA FROM PUMPS)
-ALARMS-HI /LO ,H|20, LEAK
-AC/DC POWER (2* VDC)
-OPTIONS:
 o PRINTER
 o LIGHTS, HORNS, BUZZERS, ETC.
                                          PRESSURE SENSORS

                             - INHERENT TEMPERATURE COMPENSATION
                             - COMPENSATE FOR DIFFERENCES IN SPECIFIC
                               GRAVITY OF PRODUCT
Figure 22.   MFP-414  TLG Tank Level Gauge  & Leak Detector  (50)

                   Ref:   Transitron Controls
                                     107

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     The system is equipped with a six-digit display that allows an
operator to view the total volume or weight of product in each tank in
any desired unit of measure.  A switch on the display also allows for
entering a "SLEEP" mode whereby the tank is monitored for product gain
(fill) or loss (theft or leakage).  An RS-232C port is provided for
connection to a printer, to the station computer/register, or to a
modem.  The built-in modem support allows for automatic dialing and
reporting of alarm conditions (water, leakage, theft) when equipped with
an optional modem.  This feature also provides a means of remote readout
of product inventory from a remote location.

3- TLS-150 Tank Level Sensor (Veeder-Root) (10,51)—

     The TLS-150 tank level sensor is a system designed to improve in-
ventory management of nonconductive fluids such as gasoline and diesel
fuel in underground tanks.  It can monitor up to four tanks to identify
inventory losses and accurately reconcile inventories of fuel with
dispensing and deliveries.

     This system consists of a computerized inventory monitoring with a
digital electronic sensing probe for each tank monitored.  The system
analyzes signals for liquid temperature, liquid depth, and water
level.  An integral dot matrix printer provides hard-copy documentation.

     The TLS system has three modes of operation:  leak detection, tank
inventory, and automatic delivery reporting.  When the leak monitor mode
is activated, the system continuously monitors fuel levels in each
tank.  Also, an hourly report on each tank shows temperature-compensated
inventory changes to 0.1 gallons.  When a loss of 25 gallons occurs
during a one-hour period, an inventory loss alarm initiates a signal.

     An optional telecommunications interface allows remote polling of a
TLS system from a central management location through a computer or
teletype device.

     In evaluating TLS system results, a measurement accuracy of ±1.5
degrees Fahrenheit for temperature and ±0.1 inches for level should be
assumed.  These ranges of accuracies, with tank end deflection, may
preclude low leak rate detection with the TLS system.

     Techniques to Compensate for Effects of Variables In Inventory
Control Leak Detection Tests—To minimize error when using this method
to  identify a leaking storage tank and to determine the approximate leak
rate for major leaks, the following approaches are recommended:

      1.  American Petroleum Institute publication API 1621, "Recommended
         Practice for Bulk Liquid Stock Control at Retail Outlets."

     2.  Inventory records on a daily basis.  Failure to do so  is often
         considered by a  Fire Marshall sufficient reason to order tests
                                   108

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         for leakage.   NFPA 30,  the Flammable and Combustible Liquids
         Code,  contains an inventory control  requirement.   This code has
         been adopted  by the Occupational  Safety and Health
         Administration (OSHA)  and by 35  states.

     3.   The National  Conference on Weights and Measures allows a legal
         tolerance of  0.5 percent on gasoline meters.  The total of all
         such unavoidable losses should not exceed one-half of one per-
         cent,  or five gallons  per 1,000  gallons delivered.

     4.   The system of inventory control  should detect discrepancies.

     5.   Where remote  gages are used, accuracy can be verified peri-
         odically by checking the tank with stick gages.

     6.   All tanks must be measured for water levels, especially before
         and after deliveries.   Water gaging is accomplished by applying
         a water-finding paste  to the gage stick.

Leak Effects Monitoring

     This class of leak detection methods  provides an indirect indi-
cation of leakage by evaluating resulting  environmental impact.  It may
be difficult to determine which tank is leaking when there is more than
one tank.  These methods are likely to be  more conclusive than the
quantitative testing methods, if no interfering substances are present.

1- Collection Sumps (49)—

     Collection sumps  can be used in dry hole installations as a
collection mechanism which aids in leak detection.

     In this type of system, the floor of  the storage excavation (or
secondary containment  liner) is sloped at  a rate greater than or equal
to 1/8 inch per foot to a collection sump.  The sump should be at least
two feet deep and be extended to grade via, at a minimum, a four-inch-
diameter (Schedule 40) polyvinyl chloride (PVC) pipe and topped with a
waterproof cap.  This  extension is essentially an observation well
screened in the region of the sump.  The sump should be equipped with a
removable leak detection sensor capable of detecting 1/8 inches of
standing product, which activates a strategically located aboveground
alarm when that product is present.  If constructed as described above
and shown in Figure 23, the sump and well  can also be used for leak
sampling and for the recovery of leaked or spilled product.

2- Dye Method (10)—

     In this method, a perforated pipe is  installed around the perimeter
of the underground tank storage area.  A bag of dye is connected to the
low point of the pipe.  The dye is soluble in hydrocarbon and completely
                                   109

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                                P.V.C. PIPE
                             PERFORATED P.V.C. PIPE
                             COVERED WITH
                             FIBERGLASS
                             CLOTH
                                    CAP

                               BOREHOLE ANNULU8
                                            WATER TABLE
              IMPERMEABLE PLUQ8
              PEA GRAVEL

              BOREHOLE CUTTINGS
     Source: Leak-X Corp., 560 Sylvan Ave., Englewood Cliffs, N.Y
Figure 23.  Typical Wells For Continuous Gas Or Vapor Monitoring  (49)


  Ref:  Recommended Practices for Underground Storage of Petroleum,
        New York Department of Environmental Conservation
                                110

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unaffected by water.   The bag is usually checked every day to see if any
of the dye has been dissolved.

     The installation of the perforated pipe and the length of time to
detect small leaks are the drawbacks of this system.  In addition, small
leaks most likely will not be detected.

3- Ground Water or Soil Core Sampling (10)—

     The presence of  trace organics can be detected by soil core or
water sampling in the vicinity of underground tanks.  In both cases,
small holes or wells  should be drilled.  A portable gas chromatograph
could be used to analyze samples at the site.  When a more precise
determination is required, the sample should be analyzed in a labora-
tory.  If a series of wells are drilled at proper locations, the source
of the leak may be determined.  However, this method cannot distinguish
between tank leaks and small spills in the area (usually from poor
housekeeping practices).

4- Interstitial Monitoring in Double-Walled Tanks (49)—

     Systems which monitor the interstitial space between the walls of
double-walled tanks using either vacuum sensors or fluid sensors repre-
sent the best mode of continuous leak surveillance available.  In such
systems, a leak can be detected due to failure of only one of the two
walls of the tank.  Thus, the operator can be made aware of the leak
before stored product has left the tank and entered the environment.

     In interstitial  leak monitoring system, sensors would be used to
monitor tanks that have a vacuum drawn in the space between the tank
walls.  Failure of either the inner or outer wall is detected by loss of
vacuum.  Such systems are applicable in either wet or dry hole
installations.

     Fluid sensors, on the other hand, would be located between the tank
walls to detect the presence of liquid due to failure of the inner wall
(detecting an outflow of product) or the outer wall (detecting an inflow
of water).  Such systems are more applicable in wet hole installations
where failure of the outer wall will result in the presence of a fluid
in the interstitial space.  Because failure of the outer wall can go
undetected if fluid sensors are used in dry hole installations, such an
application is not recommended if pressure sensors can be used instead.

     In the case of either type of interstitial monitoring system, it is
important that the tank be constructed to allow for free movement of
fluids or gases in the space between the tank walls so that a leak any-
where in the tank can activate strategically located sensors.
                                   Ill

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5- LASP Monitoring System (Leakage Alarm System for Pipe) (52)—

     The wall-diffusion effect is the basis for the Leakage Alarm System
for Pipe (LASP) system.  A one-half-inch-diameter sensor tube is made of
a plastic material that allows rapid wall diffusion.  The LASP system
consists of three components:   a flexible sensor tube, a pump, and a
detector.  The sensor tube can be moved to strategic locations around
the tank.  The vapors of a leaked product coming in contact with the
LASP tube will diffuse into the tube and be captured.  At regular
intervals (e.g., every 24 hours), a stream of air followed by an injec-
tion of a detectable vapor is  pumped through the LASP tube.  The
detector at the end of the LASP tube will register on a line recorder
any leakages carried by the air stream, and the regular injection of a
detectable vapor will show as  an end peak.

6- Observation Wells (49)—

     Observation wells are used to monitor for leaks from underground
tank installations in areas of high ground water.  In this instance,
ground water will be present in the excavation for most or all of the
year.  A diagram of an observation well installation is shown in Figure
24.

     An observation well, or liquid product sensing well, consists of,
at a minimum, a four-inch-diameter (Schedule 40) PVC pipe placed in the
tank excavation.  The wells are constructed with a well screen long
enough to provide a length of five feet or more above the water table',
or to the well cap, and extending a minimum of five feet into the ground
water or two feet below the tank bottom, whichever is greater.  Well
screens typically have a slot size of 0.02 inches.  The connecting well
pipe is extended to grade and covered with a waterproof cap which is
capable of being sealed.

     As is true of the vertical section of the U-tube, if observation
wells are constructed as described above and shown in Figure  24, they
can be used for leak sensing, direct sampling, and product (and con-
taminated ground water) recovery.  When leak sensors are used, they must
be capable of detecting a 1/8-inch layer of the stored product on the
ground water surface, and they must activate a strategically  located
aboveground alarm when that product is detected.

     The selection of the number and location of the observation wells
in a particular storage system  is dependent upon the local hydrogeology,
including parameters such as  the ground water flow direction.  It is
recommended that any installation using observation wells  employ at
least two wells in each excavation.

     Existing  sites may have  observation wells drilled to  ground water,
provided the  location  and orientation  of  the tanks and piping is known.
                                   112

-------
     EACH WELL CONSISTS OF 4* PERFORATED PVC PIPE, DRIVEN AT
     LEAST 2  FEET BELOW THE  BOTTOM OF THE  TANK  OR AT LEAST
                    5 FEET INTO THE QROUNDWATER
WATERPROOF
CAPS CAPABLE OF
BEING SEALED
        \
OVERFILL PREVENTION       MANWAY- ALLOW ENTRY
DEVICE  WITH  EXTRACTABLE  |NTO THE TANK- EXTENSION
TEE TO  GRADE FITTING     TO GRADE (OPTIONAL)  FITTING

                               FINISHED GRADE
                  QROUNDWATER
                T&
                                                           >-TCJ
                                          ONCRETE KNOCKOUT
                                        SECTION (OPTIONAL)
                                     SPACING AND FILL TO
                                     BE IN ACCORDANCE TO
                                     TANK  MANUFACTURER
                                     SPECIFICATIONS
                                    6'MIN.
        i—f i        unuunuTTA i en  —  i
     ' J7*                  -  V  *         ZIr-

 Source. James Pirn Suffolk County Dept. of Health Services
                                           T
                                        -V
     Figure 24.   Examples Of Observation Wells (49)

     Ref:   Recommended  Practices for Underground Storage of Petroleum,
           New York Department of Environmental Conservation
                                  113

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7- Pollulert and Leak-X Detection Systems (11,53,54)—

     Both detection systems use the significant difference between the
thermal conductivity of hydrocarbons and of water to detect leaks.  The
system's solid-state electronic sensors are placed in a well near the
storage tank.  The bottom of the well should be at least 10 feet below
the bottom of the storage tank.  A programmed microprocessor contin-
uously monitors the presence of water or hydrocarbons in the monitoring
well.  If the sensors detect any hydrocarbons, an alarm sounds.  The
unit can be wired to automatically summon personnel by telephone.

     The major drawbacks of this method are the installation and expense
of the monitoring well.  However, once the well is installed, if a tank
begins to leak, the leak is detected before major damage occurs (unless
the leak goes straight down, as happens when ground water is low).

8- Remote Infrared Sensing (10)—

     This method depends on the difference in soil temperature due to
the presence of hydrocarbons.  An infrared sensing device (either an
infrared camera or a video system) remotely senses temperatures in the
storage tank area.  This is usually done from an aircraft rather than at
ground level.

     This method is usually only a part of a survey for leak detection;
additional ground or subsurface information is required to complete the
survey.  The ability of this method to detect small leaks is doubtful.

9- Surface Geophysical Methods (10)—

     The presence of hydrocarbons in the ground could be determined by
using a geophysical method such as ground penetrating radar, electromag-
netic induction, or resistivity techniques.  These methods are not the
primary subject of this text; therefore, they will not be discussed in
further detail.

10- U-Tubes (49)—

     A U-tube consists of a four-inch-diameter (Schedule 40) PVC pipe
installed as shown in Figure 25.  The horizontal segment of the pipe is
half-slotted (typical slot size, 0.06 inches), wrapped with a mesh cloth
to prevent backfill infiltration, and sloped (pitched) toward the sump
with a slope on the order of 1/4 inch per foot.  At the higher end of
the pipe, there is a 90-degree sweep to a vertical pipe that is extended
to grade.  At the lower end of the horizontal pipe, there is a tee
connection with a vertical pipe.  Above the tee this vertical section is
extended up to grade, and below the tee it is extended down two feet to
act as a collection sump.  All vertical pipe sections are unperforated,
and the bottom of the sump is sealed to be leakproof.  All openings to
grade are provided with watertight caps capable of being sealed.  It is
                                   114

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    FINISHED
     GRADE -
                      OVERFILL
                     PREVENTION
                     DEVICE WITH
                    EXTRACTABLE
                    TEE TO GRADE
OBSERVATION WELLS: WATERPROOF CAPS
                      CAPABLE OF BEING
                      SEALED
       EXTENSION OF
     MANWAY TO GRADE
        (OPTIONAL)
                                                                 NOTE:ALL PIPING
                                                                       TO BE 4'
                                                                       SCHEDULE
                                                                       40 PVC
     4' TEE
    SEALED
      CAP -
                                                                   90*  SWEEP
    4* DIAMETER  HALF SLOTTED PIPE
    WRAPPED  WITH  FILTER MATERIAL - I/4"PER
    FOOT PITCH  TOWARDS SUMP.
    SLOT SIZE .060
                                  -SPACING  AND FILL TO BE IN ACCORDANCE TO
                                  TANK  MANUFACTURER  SPECIFICATIONS
Source: James Pirn, Suffolk County Dept. of Health Services
              Figure  25.   Example Of A U-Tube  Installation (49)

       Ref:  Recommended  Practices for Underground Storage of Petroleum,
             New York Department of Environmental  Conservation

-------
imperative that these tubes be secured so that products cannot be
accidentally delivered into them.

     These tubes may be installed under each tank in an excavation, or
centrally located in the excavation.  In either case, the excavation
bottom must be sloped slightly (a minimum of 1/4 inch per foot) toward
the U-tube to permit collection of any leaked material.

     The collection sump of the U-tube should be equipped with a
removable sensing device which is capable of detecting 1/8 inch of
standing product or a 1/8-inch layer of product on water.  This sensing
device is installed so as to activate an alarm which is strategically
located aboveground.

     If the vertical section of the U-tube is designed as described
above and shown in Figure 25, leaked or spilled product can be readily
recovered from the collection sump using standard equipment such as a
3-3/8-inch submersible pump.  Construction of the vertical section in
this manner also permits easy sampling of leaked material to pinpoint
the source of a leak. This may be necessary in situations where two or
more similar products are stored, such as in an excavation housing both
leaded and unleaded gasoline.

     U-tubes can be used only in situations where the excavation is
above the high level mark of the ground water table (dry hole
installations), the excavation has been provided with an impervious
secondary containment layer on its floor, and the installation is
covered with a waterproof cap.  In such cases, any leaked material will
eventually find its way to the U-tube's collection sump where  it can be
detected without water interference.

11- Vapor Wells (49)--

     A vapor well  is similar to an observation well except that it is
intended for monitoring vapors or odors from underground storage systems
instead of liquids.  Such a well consists of a four-inch-diameter PVC
pipe (Schedule 40)  installed in the excavation within  five feet of the
tank.  In dry  installations, these wells extend to the containment liner
on the floor of the excavation.  In wet installations, they extend into
the ground water.

     The well  screens in vapor wells  should have a slot  size of 0.02
inches.  In dry hole installations, the screened opening should extend
from the containment volume  floor to  a height of at  least five feet.  In
wet hole installations, the  well screen must be long enough to provide a
length of five  feet or more  above the water table and  should extend a
minimum of five feet into  the water table or two feet  below the tank
bottom, whichever  is greater.
                                   116

-------
     Vapor wells can be used only at uncontaminated sites.  Once product
vapors have entered the well, they will remain there until both their
source has been removed (the leak has been pinpointed and repaired) and
the well has been purged free of residual vapors.  If the well cannot be
purged, the vapor well must be either retrofitted with an alternate
means of sensing leaked product or abandoned.  Figure 23 is a diagram of
a typical, dry hole, vapor well.
                                   117

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                              REFERENCES
 1.   Conference Report on H.R. 2867  Hazardous  and  Solid  Waste  Amendments
     of  1984,  Congressional Record-House,  H11140,  October  3,  1984.

 2.   National  Petroleum News, January  1979,  pp.  64.

 3.   National  Fire  Protection Association, Underground Leakage of  Flam-
     mable  and Combustible Liquids,  NFPA 329,  National Fire  Protection
     Association, Batterymarch Park, Quincy, MA  02269, 1983.

 4.   Heath  Consultants, Inc., Petro  Tite Tank  Tester  Bulletin, Heath
     Consultants, Inc., Stoughton, MA.

 5.   Tightness-Testing Systems for Underground Tanks  Symposium,
     Petroleum Equipment Institute,  Las  Vegas, Nevada, Sept.  28,  1983.

 6.   Description  of Ainlay Tank  Tegrity  Testing  (TTT), draft  report from
     Steel  Tank Institute  (STI),  Northbrook, NJ.

 7.   Underground  Fuel Tanks!  Regulatory and Remedial Outlook Symposium,
     USEPA, Arlington, VA, July  9-10,  1984.

 8.   Verbal Communication with John  Ainlay,  STI, North'brook,  IL.

 9.   Technology for the Storage  of Hazardous Liquids, A  State-of-the-Art
     Review, New  York State Department of Environmental  Conservation,
     Albany, NY,  Jan. 1983.

10.   Methods for  Detecting Leaks in  Underground  Storage  Tanks, Draft
     Report, Environmental Protection  Agency,  Office  of  Toxic
     Substances,  Washington D.C. 1984.

11.   Pollution Engineering, July 1984.

12.   ARCO Petroleum Products  Co., ARCO Underground Tank  Leak Detector
     Bulletin, ARCO Petroleum Products,  Harvey Technical Center,  Harvey,
     IL.

13.   Verbal Communication  with  Gary  L. Everett,  ARCO  Petroleum Products,
     Harvey, IL.

14.   Certi-Tec Tank Testing  System Description,  Fuel  Recovery Company,
     Environmental  Services,  Inc.,  St. Paul, MN

15.   Verbal Communication  with Jonathan  Nedved,  Fuel  Recovery Company,
     Environmental  Services,  Inc.,  St. Paul, MN.
                                   118

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16.  "Ethyl" Tank Sentry Testing Bulletin, Ethyl Corporation, Petroleum
     Chemicals Division, Houston, TX.

17.  Verbal Communication with A. V. Morschauser, Ethyl Corporation, Pe-
     troleum Chemical Division, Houston, TX.

18.  Horner EZY-CHEK Leak Detector Bulletin, Horner Creative Metals,
     Inc., Kawkawlin, MI.

19.  Horner EZY-CHEK Leak Detection System Bulletin, Horner Creative
     Metals, Inc., Kawkawlin, MI.

20.  Verbal Communication with John Horner, Horner Creative Metals,
     Inc., Kawkawlin, MI.

21.  Verbal Communication with Jack Stillwagon, Heath Consultants, Inc.,
     Belle Vernon, PA.

22.  Helium Differential Pressure Testing, Report, IT Corporation, Mar-
     tinez, CA.

23.  Verbal Communication with Mr. Schweizer, IT Corporation, Martinez,
     CA.

24.  Leak Lokator Bulletin, Hunter Environmental Services, Inc.,
     Malvern, PA.

25.  Verbal Communication with Donna Hymes, Hunter Environmental
     Services, Inc., Malvern, PA.

26.  Mooney Tank Test Detector Description, Mooney Equipment Co., Inc.,
     New Orleans, LA.

27.  Verbal Communication with Joseph R. Mooney, Mooney Equipment Co.,
     Inc., New Orleans, LA.

28.  PACE Tank Tester, Report, Petroleum Association for Conservation of
     Canadian Environment (PACE), Ottawa, Canada, April 1985.

29.  Underground Tank Testing Symposium, Petroleum Association for Con-
     servation of the Canadian Environment (PACE), Toronto, Ontario, May
     25-26, 1982.

30.  Tank Auditor Method of Leak Detection, Report, WEB Engineering
     Associates, Inc., Leak Detection Services, Hingham, MA.

31.  Verbal Communication with William E. Baird, WEB Engineering Associ-
     ates, Inc., Leak Detection Services, Hingham, MA.
                                  119

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32.  Maresca, J. W. and P. C. Evans, "Measurement of Leaks in
     Underground Storage Tanks Using Laser Interferometry," Technical
     Report No. 1,
     SRI Project 7637, SRI International, Menlo Park, CA, June 1979.

33.  Maresca, J. W., P. C. Evans, R. A. Padden, and R. E. Wanner,
     "Measurement of Small Leaks in Underground Gasoline Storage Tanks
     Using Laser Interferometry," Final Report, SRI Project 7637, SRI
     International, Menlo Park, CA, Sept. 1981.

34.  Verbal Communication with Joseph W. Maresca, Vista Research, Inc.,
     Palo Alto, CA.

35.  Oh, C.B., Acoustical Monitoring System (AMS), Description Letter,
     KEP Corp. Knoxville, TN.

36.  Ultratest Helium Mass Spectrometer Leak Detector Bulletin, Leybold-
     Heraeus Vacuum Products, Inc., Export, PA.

37.  Detection of Leaks from Underground Tanks and Pipes Using Helium
     Gas, Report, Smith and Denison, Hayward, CA.

38.  Verbal Communication with William Burkhart, Smith & Denison,
     Hayward, CA.

39.  TRC Leak Detection, Tracer Research Corporation, Tucson, AZ.

40.  Ultrasonic Leak Detection-Ultrasound, Report, Ue Systems, Inc.,
     Elmsford, NY.

41.  Power Engineering, April 1984, pp, 52-53.

42.  Plant Engineering, April 3, 1980, pp. 103-106.

43.  Hydrocarbon Processing, Jan,  1983, pp. 93-94.

44.  Verbal Communication with Mark A. Goodman, Ue Syscems, Inc.,
     Elmsford, NY.

45.  Tanknology Bulletin, Tanknology,  Edmonton, Alberta.

46.  Verbal Communication with Edward  Smith, Tanknology, Edmonton,
     Alberta.

47.  Varian Helium Leak  Detectors  938-41 and SPY  2000 Bulletin,  Varian,
     Vacuum  Products  Division, Lexington, MA.

48.  Verbal  Communication with Ert  Shivert, Varian,  Vacuum Products
     Division,  Lexington, MA.
                                   120

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49.  Recommended Practices for Underground Storage of Petroleum, New
     York Department of Environmental Conservation, Albany, NY, May
     1984.

49a. Comments on "More About Leaking Underground Storage Tanks:  A
     Background Booklet to Accompany the Chemical Advisory," Report,
     Holland & Knight, Washington, D.C., September 1984.

50.  MFP-414 Leak Detector Bulletin, Transitron Controls, Easton, MA.

51.  TLS-150 Tank Level Sensor, Bulletin, VEEDER-Root, Petroleum
     Products, Hartford, CT.

52.  Leakage Alarm System for Pipe (LASP) Bulletin, Teledyne Geotech,
     Garland, TX.

53.  Pollulert Fluid Detection Systems Bulletin, Mallory, Electrical/
     Electronic Group of Emhart, Indianapolis, IN.

54.  Leak-X Bulletin, Leak-X Corp, Englewood Cliffs, New Jersey.

55.  Recommended Practice for Bulk Liquid Stock Control at Retail
     Outlets, Publication 1621, American Petroleum Institute,
     Washington, DC, 1977.
                                   121

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                                     APPENDIX
                              LEAK DETECTION METHODS
                    MANUFACTURER OR PRACTITIONER PHONE NUMBERS
LEAK DETECTION TESTING METHODS
  PHONE NUMBER
                    CONTACT NAME
Volumetric (Quantitative) Leak
Testing Methods
   1 - Ainlay Tank Tegrity Testing
       (TTT)
   2 - ARCO HTC Underground Tank
       Leak Detector
   3 - Certi-Tec Testing
   4 - "Ethyl" Tank Sentry Testing
   5 - EZY-CHEK Leak Detector
   6 - Fluid-Static (Standpipe)
       Testing
   7 - Heath Petro Tite Tank and
       Line Testing (Kent-Moore
       Testing)
   8 - Helium Differential Pressure
       Testing
   9 - Leak Lokator Test (Hunter-
       Sunmark Leak Detection)
  10 - Mooney Tank Test Detector
  11 - *PACE Tank Tester
  12 - *PALD-2 Leak Detector
  13 - Pneumatic Testing
  14 - Tank Auditor
  15 - *Two-Tube Laser
       Interferometer System
(312) 328-6119    Mr. John Ainlay

(312) 333-3000    Mr. Gary L. Everett

(612) 487-1484    Mr. Jonathan Nedved
(609) 452-8600    Mr. A. V. Morschauser
(517) 684-7180    Mr. John Homer
Method is used by different contractors
(617).344-1400    Mr. Jack Stillwagon
(415) 228-8400    Mr. John Schweizer
(215) 296-7380    Mrs. Donna Hymes
(504) 241-0453
(416) 443-7032
                  Mr. Joseph Mooney
                  Mr. Jack Witherspoon
(Not Available)   Mr. Werner Grundmann
3425 West 30th Ave.
Vancouver, B.C.,
V6S1W3 CANADA
Method is used by different contractors
(617) 740-1717    Mr. William E. Baird
(415) 424-1251    Mr. Joseph W. Maresca
 Not commercially available.
                                     A-l

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LEAK DETECTION TESTING METHODS
   PHONE NUMBER
   CONTACT NAME
Nonvolumetrie (Qualitative) Leak
Testing Methods
   1 - *Acoustical Monitoring
        System (AMS)
   2 - Leybold-Heraeus Helium
         Detector, Ultratest M2
   3 - Smith & Denison Helium Test
   4 - TRC Rapid Leak Detector for
       Underground Tanks and Pipes
   5 - *Ultrasonic Leak Detector,
        Ultrasound
   6 - VacuTect (Tanknology)
   7 - Varian Leak Detector
Inventory Monitoring
   1 - Gage Stick
   2 - MFP-414 Leak Detector
   3 - TLS-150 Tank Level Sensor
       (Veeder-Root)
Leak Effects Monitoring
   1 - Collection Sumps
   2 - Dye Method
   3 - Ground Water or Soil Core
       Sampling
   4 - Interstitial Monitoring  in
       Double-Walled  Tanks
   5 - L.A.S.P. Monitoring  System

   6 - Observation Wells
   7 - Pollulert  and  Leak-X
       Detection  Systems
(615) 966-4773    Mr.  Charles B. Oh
(412) 327-5700

(415) 782-9788

(602) 623-0200
Mr. William C.
Worthington
Mr. William H.
Burkhart
Mr. Glenn Thompson
(914) 592-1220    Mr. Mark A. Goodman

(403) 483-3506    Mr. Edward Adams
(617) 935-5185    Mr. Roger Schneider

Method is used by different contractors
(617) 238-6911    Mr. Stanley Hayes
(203) 527-7201    Mr. Tony Spera
Method is used by different contractors
Method is used by different contractors
Method is used by different contractors

Method is used by different contractors

(214) 271-2561    Industrial  System Mar-
                  keting
Method is used by different contractors
(317) 856-3857    Mr. Dale McClain  (Pol-
                  lulert)
(212) 822-6767    Mr. John Gelles
                  (Leak-X)
  Not commercially available.
                                      A-2

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LEAK DETECTION TESTING METHODS
   PHONE NUMBER
CONTACT NAME
   8 - Remote Infrared Sensing
   9 - Surface Geophysical Methods
  10 - U-Tubes
  11 - Vapor Wells
Method is used  by different contractors
Method is used  by different contractors
Method is used  by different contractors
Method is used  by different contractors
*Not commercially available
                                      A-3
                                                        ft US GOVERNMENT PRINTING OFFICE 1986 - 646-116/20741

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