United States
Environmental Protection
Agency
Office of Research and
Development
Washington DC 20460
Technology Transfer
             EPA/625/5-86/020
Nitrogen Oxide Control
for Stationary
Combustion Sources

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                                 EPA/625/5-86/020
                                     July 1986
   Nitrogen Oxide Control for
Stationary Combustion Sources
         Office of Research and Development
        U.S. Environmental Protection Agency
             Cincinnati, OH 45268

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                                Notice

This document  has been  reviewed in accordance with the U.S.  Environmental
Protection Agency's peer and  administrative review policies and approved for
publication. Mention of trade names or commercial products does not constitute
endorsement or  recommendation for use.

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                              Contents

Chapter                                                          Page

 1  Introduction	     1

    1.1   Background 	     1
    1.2   NOX Emission Regulations	     1
    1.3   Mechanisms of NOX Formation  	     3
    1.4   General Schemes for NOX Reduction	     4
    1.5   NOX Emission Sources Considered in This Document	     5
    1.6   Organization of This Document	     8

 2  NOX Control Alternatives 	    11

    2.1   Introduction 	    11
    2.2   Precombustion Control Technologies	    11
    2.3   Combustion Modification Technologies	    11
    2.4   Postcombustion Technologies	    20
 3  Performance and Cost Data: Utility and Large Industrial Boilers	    23

    3.1   Introduction 	    23
    3.2   Coal-Fired Boilers	    23
    3.3   Oil- and Gas-Fired Boilers	    34

 4  Performance and Cost Data: Packaged Boilers Firing Oil or Gas	    39

    4.1   Introduction 	    39
    4.2   Reduced Combustion Air Preheat	    39
    4.3   Flue Gas Recirculation	    39
    4.4   Low NO* Burners	    39
    4.5   Other Technologies	    40

 5  Performance and Cost Data: Gas Turbines and  Stationary
    Reciprocating Engines 	    41

    5.1   Introduction 	    41
    5.2   Gas Turbines	    41
    5.3   Stationary Engines	    42

 6  References	    47

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                               Figures

Number                                                          Page

1-1   Basic Mechanism of NOX Formation	    3
1-2   General Schemes for NOX Reduction	    4
1-3   Classification of Coal-Fired Boilers	    6
1-4   Utility Boiler Firing Configurations for Pulverized Coal	    6
1-5   Main Types of Stokers Used in Industrial Boilers	    7
1-6   Front View of Circular Burner Used for Oil Combustion	    7
1-7   Front View of Cell Burner Used for Gas Combustion	    7
1-8   Pulverized Coal-Fired Boiler Employing Horizontally
     Opposed Burners	    8
1-9   Simple-Cycle Turbine	    9

2-1   Typical Staged Combustion: Overfire Air	   13
2-2   Arch-Fired Boilers	   14
2-3   Three Temperature Reduction Methods for Boilers	   14
2-4   Low NOX Burner: Staged-Air Design 	   15
2-5   Low NOX Burner: Staged-Fuel Design	   15
2-6   Low NOX Burner: Foster Wheeler Controlled Flow/Split
     Flame Burner	   16
2-7   Low NOX Burner: Babcock & Wilcox Dual Register
     Burner / Compartmented-Windbox System	   17
2-8   Low NOX Burner: Riley Stoker Controlled Combustion
     Venturi Burner	   17
2-9   Low NOX Burner: Riley Stoker Directional Flame Burner	   18
2-10 Low NOX Burner: EPA Distributed Mixing Burner	   18
2-11 Low NOX Burner: Combustion Engineering Low NOX
     Concentric Firing System	   19
2-12 In-Furnace Destruction by Mitsubishi Advanced Combustion
     Technology (MACT) Process	   19
2-13 NOX Reduction Options for Stationary Engines	   19
2-14 Classification of NOX Flue Gas Treatment Processes 	   20
2-15 Typical Flow Diagram for Selective (Ammonia) Catalytic
     Reduction Process 	   21
2-16 Thermal DeNOx System — Process  Flow Diagram	   21

3-1   NOX Reduction by BOOS for Single Wall-Fired Boilers
     Burning Coal at 120 Percent Excess Air	   24
3-2   NOX Reduction by BOOS for Horizontally Opposed Wall-
     Fired Boilers Burning Coal	   24
3-3   NOX Reduction by BOOS for Tangential-Fired Boilers
     Burning Coal	   25
3-4   Typical Retrofit Arrangement for Overfire Air	   25
3-5   NOX Reduction by Overfire Air for Tangential-Fired
     Boilers Burning Coal	   26
3-6   Costs of Retrofitting Coal-Fired Boilers for Overfire Air	   26
3-7   Pilot-Scale Test Results for the CCV Burner	   27
3-8   Theoretical IMOX Emissions Versus Burner Stoichiometry
     for the Controlled Flow/ Split Flame Burner	   27

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                         Figures (continued)

Number                                                           Page
3-9  NOX Emissions for Dual Register Versus Circular
     Burners in Coal-Fired Boilers	   28
3-10 Pilot-Scale Results for NOX Reduction by Low NOX
     Cell Retrofit Burners	   29
3-11 NOX Emissions for the Low NOX Concentric Firing
     System in Coal-Fired Tangential Boilers: No Overfire Air	   29
3-12 NOX Emissions for the Low IMOX Concentric Firing
     System in Coal-Fired Tangential Boilers: Full Overfire Air	   29
3-13 Offsetting Retrofit Costs of Controlled  Flow/Split Flame Burners
     with Oil Savings	   30
3-14 NOX Reduction by MACT for a 600-MW Coal/Oil Boiler	   31
3-15 NOX Emissions from a Slagging Combustion Pilot Plant
     Firing Coal 	   31
3-16 NOX Emissions from a Slagging Combustion Pilot Plant
     Firing Coal, Oil, and Mixtures	   32
3-17 Test Results for SCR on a Coal-Fired Boiler	   32
3-18 Incremental Capital Cost of SCR and Other NOX Control
     Technologies for a New Tangential-Fired Boiler	   33
3-19 NOX Reduction Due  to Flue Gas Recirculation in a Stoker-
     Fired Boiler	   34
3-20 NOX Reduction by Lowering Excess Air in a Gas-Fired
     Utility Boiler	   34
3-21 NOX Reduction by BOOS for a Gas-Fired Utility Boiler	   35
3-22 NOX Reduction by SNR for Oil-Fired Utility Boiler	   36

5-1  NOX Reduction by Water or Steam Injection: Gas Turbine
     Firing Natural Gas	   41
5-2  NOX Reduction by Water or Steam Injection: Gas Turbine
     Firing Distillate Oil	   41
5-3  Performance of Selective Catalytic Reduction on  a Gas
     Turbine	   42
5-4  NOX Reduction by Water/ Fuel Emulsion for Diesel Engine	   43
5-5  NOX Reduction by Water/ Fuel Emulsion for Diesel Engine	   43
5-6  NOx Reduction by Exhaust Gas Recirculation for  Diesel
     Engine	   44
5-7  Effect of Lean-Burning Torch Ignition on Spark-Ignition
     Gas-Fired Engine	   44
5-8  NOX  Reduction by Charge Cooling for a Spark-Ignition
     Gas-Fired Engine	   45
5-9  NOX Reduction by Selective Catalytic Reduction for
     Spark-Ignition Engine	   46
5-10 NOX Reduction by Selective Catalytic Reduction:  Long-
     Term Test for Spark-Ignition Engine	   46

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                                 Tables

Number                                                           Page

1-1  Stationary Sources of NOX	    1
1-2  New Source Performance Standards for NOX Emissions from
     Utility Boilers	    1
1-3  Proposed New Source Performance Standards for NOX Emissions
     from Industrial Boilers	    2
1-4  New Source Performance Standards for Stationary Gas
     Turbines	    2
1-5  Typical Nitrogen Content of Selected Fuels	    3
1-6  Characteristics of Stationary Reciprocating Engines  	    9

2-1  Combustion Modification Technologies	   12

3-1  Average Reported NOX Reduction with Low Excess Air Firing
     in Coal-Fired Utility Boilers	   23
3-2  Average Reported NOX Reduction with Overfire Air Firing in
     Tangential Coal-Fired Utility Boilers	   26
3-3  Cost of Retrofitting Coal-Fired Boilers for Overfire Air	   27
3-4  NOX Performance for PM  Burner System in Tangential-Fired
     Boilers	   30
3-5  Cost of Retrofitting with PM Burners	   30
3-6  Capital Cost and Cost-Effectiveness of Thermal DeNOx Process	   33
3-7  Economic Evaluation of SCR for Coal-Fired Utility Power
     Plants: 80 Percent NOX Removal	   33
3-8  NOX Removal in Oil-Fired Industrial Boilers with Selective
     Catalytic Reduction	   36
3-9  Annual Operating Cost Estimates for Thermal DeNOx on a
     200,000 Ib/h Oil-Fired Industrial Boiler	   37
3-10 Capital and Operating Cost Data for Selective Catalytic
     Reduction Systems for Oil-Fired and Gas-Fired Boilers	   37

4-1  NOX Emission Performance for Low NOX Burners in Single-
     Burner Oil- and Gas-Fired Boilers	   39
4-2  NOX Emission Reduction for Gas-Fired Fire-Tube Boiler with
     a "Fiber" Low NOX Burner	   40

5-1  NOX Reduction by Exhaust Gas Recirculation: Natural
     Gas Spark-Ignition Engines	   44
5-2  NOX Reduction by Ignition Retard: Natural Gas-Fired
     Engines	   45
5-3  NOX Reduction by Selective Catalytic Reduction for
     Diesel Engine	   45
5-4  Capital Costs for SCR Systems for Lean-Burn Spark-
     Ignition Engines	   46
5-5  NOX Reduction by NCR: Results for Tests of 13 Rich-
     Burn Spark-Ignition Engines	   46
5-6  Cost of NCR Systems for Rich-Burn, Spark-Ignition Engines	   46

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                         Acknowledgments

Several individuals contributed to the preparation and review of this document. It
was written by Thomas Beggs, JACA Corporation, Fort Washington, Pennsylvania.
Robert E.  Hall,  J. David  Mobley, and James A.  Eddinger were the  U.S.
Environmental Protection Agency reviewers. Other reviewers were Gary Bisonett,
Pacific Gas  & Electric Co., San  Francisco;  John  Maulbetsch,  Electric Power
Research Institute, Palo Alto,  California; F.  Richard  Kurzynske,  Gas Research
Institute,  Chicago; and  Howard Mason,  Acurex Corporation, Mountain View,
California.  The  Contract  Project   Officer was  Norman  Kulujian,  Center  for
Environmental Research Information,  U.S.  Environmental Protection Agency,
Cincinnati, Ohio.
For additional information on nitrogen oxides control alternatives, contact:
            Combustion Research Branch
            Air and Energy Engineering Research Laboratory
            U.S. Environmental Protection Agency
            Research Triangle Park, NC 27711

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                                                Chapter 1
                                               Introduction
1.1    Background
Nitrogen dioxide is a criteria pollutant under the Clean
Air Act. Accordingly, nitrogen oxide emissions (notably
nitrogen dioxide and nitric oxide, usually referred to as
NOX) are considered a major environmental concern.
Most NOX emissions result from fossil fuel combustion.
Mobile sources  of combustion, mainly motor vehicles
and  aircraft, contributed about 45 percent of total 1980
NOx emissions nationwide.(1) Stationary sources, con-
tributing about 55 percent, are covered in detail in this
document.(1)  Table 1-1 characterizes  NOX  emissions
from stationary sources.

Table 1-1.   Stationary Sources of NOX (1)
Source
Utility boilers
Industrial boilers
Gas turbines
Stationary engines
Miscellaneous
Total
Approximate
No. of
Sources
2,000
6,000



Appropriate
Size Range
MW
40-1,000
10-200
10-1,000
0-0.1

Total
NOX, %
53
14
2
20
11
100
This document  covers  the  first four sources listed in
Table 1-1, which together represent about 90 percent of
all stationary source emissions of NOX. This provides in
one publication the  basic information  needed  by
managers and others who are involved with the major
stationary sources of IMOX emissions to make prudent
decisions for controlling these emissions to meet  ap-
plicable  regulations.  The document provides a
technology overview for managers of power plants and
other stationary sources; state and local air pollution
agency personnel charged  with  monitoring the  com-
pliance status of sources; and vendors and consultants
actively  engaged in developing  equipment, systems,
and approaches for reducing stationary source emis-
sions of NOX. The goal  is not necessarily to provide all
the information necessary to make a final decision on a
means  of NO* control,  but rather  to present  the
available  options with a   brief assessment  of  the
achievable results and,  where it  exists, the cost of  the
options.

1.2  NOX  Emission Regulations
The development of control  technologies for stationary
sources of NOX has,  in large measure, resulted in emis-
 sion regulations for new sources that are based on the
 reduction  achievable by these  demonstrated  tech-
 nologies. In order to fully appreciate the later discus-
 sions of these technologies  it is appropriate to review
 the regulations that must be met by the various source
 categories.

 Utility boilers, which represent the largest stationary
 source sector, have been regulated at the Federal level
 since  1971. The New Source Performance Standards
 (NSPS) have since been revised as shown in Table 1-2,
 which lists the  NOX  requirements of the  1978 NSPS.
 Note that the  highest  emission  limits are for coal,
 reflecting the relative difficulty of NOX removal from
 coal burning  as discussed in detail  later in this docu-
 ment. Note also that emission limitations for synthetic
 fuels are in general  higher  than for their fossil fuel
 counterparts due to the higher fuel nitrogen content.


 Table 1-2.    New Source Performance  Standards for  NOv
                                                                   Emissions from Utility Boilers'
                                                                                            ,a,b
                                                                        Fuel
                                       Emission Limit,
                                      ng/J (lb/106 Btu)
 Bituminous and anthracite coal, certain          260 (0.60)
 lignites, and solid fuels not elsewhere
 classified'1'''
 Subbituminous coal and coal-derived fuel        210 (0.50)
 Distillate and residual oil                     130 (0.30)
 Coal-derived oil and shale oil                  210 (0.50)
 Natural gas                                86 (0.20)
 Coal-derived gas	210 (0.50)
 "Source: 40 CFR, Part 60, Subpart Da.
 hApplies to units for which construction commenced after September
 18, 1978, and which are capable of combusting more than 73 MW
 (250 x 10- Btu/h).
 'Lignites meeting certain conditions of source and type of combustion
 have an emission limit of 340 (0.80).
 rfSolid fuels containing  more than 25 weight percent coal refuse are
 exempt from the NOX standard.


The relative stringency of the  1978 NSPS  is  largely
responsible  for the recent efforts to develop so-called
low NOX  burners,  which constitute a  major control
technology, as discussed later, and which are designed
to significantly reduce  NOX emissions. Also because of
these requirements, most of the results presented in
later sections are  in  terms  of percent reduction  of
NOX. An NSPS for  paniculate matter and N0xwas pro-
posed for industrial boilers in  June 1984 (Table  1-3).
                                                    1

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Under a court order, EPA  is required to promulgate
regulations by November 1986. Industrial boilers that
were placed in operation after June 1984 are subject to
the standards. Again the limitations vary with  fuel type
and, in this case, within fuel type by method of combus-
tion or fuel nitrogen content.  The final regulation may
differ from that summarized in Table 1-3 but is expected
to be applied retroactively to June 1984.
 Table 1-3.
Proposed New Source Performance Standards
for NO, Emissions from Industrial Boilers"'6 c
                  Fuel
                           Emission Limit,
                          ng/J (lb/106 Btu)
 Coal, pulverized                             301 (0.70)
 Coal, mass-feed stoker                        215 (0.50)
 Coal, spreader stoker and fluidized bed           258 (0.60)
 and certain lignites'*
 Distillate oil                                 43  (0.10)
 Residual oil > 0.35 weight percent nitrogen        172 (0.40)
 Residual oil < 0.35 weight percent nitrogen        129 (0.30)
 Natural gas                                  43 (0.10)
 Mixtures of natural gas or distillate oil            129 (0.30)
 with wood or solid waste	
 "Source: 40 CFR, Part 60, Subpart Db.
 'Applies to units for which construction commenced after June 19,
 1984, and which are capable of combusting more than 29 MW (100 x
 10" Btu/h).
 cThe standard includes a formula for the emission limit for mixtures of
 coal, oil, or natural gas with any other fuel except the special category
 of lignite.
 dLignites meeting certain conditions of source and type of combus-
 tion have an emission limit of 340 (0.80).
 The  NSPS  for  stationary gas  turbines, as shown in
 Table 1-4, is more complicated than the new source
 standards for boilers. NOX emission limitations under
 this standard are  determined by one of two formulas
 depending on the size of the unit, with a stricter limit for
 larger turbines. Each  formula includes an allowance for
 heat rate (the  lower the heat rate, the  greater  the
 allowable emissions)  and a term (F) for nitrogen con-
 tent.  Note  that F applies for  fuel nitrogen contents
 greater than 0.015 percent and  varies as a gradually in-
 creasing function  of  nitrogen content (N) up to N =
 0.25, above which F is constant at 0.005.
 The control of NOX emissions from stationary sources
 may also be regulated at the Federal level by the Preven-
 tion  of Significant Deterioration  (PSD) and Emission
 Offset (EO)  programs. Under PSD, siting a new source
 may be contingent upon meeting specified air quality
 impact limits. Therefore, if the ambient  NOX concentra-
 tion attributable to a  source is limited, an effective limit
 is placed on the  actual emissions from that  source.
 Under EO,  the  NOX  emissions  from a  source may be
 voluntarily  controlled to a stringent  level in  order to
 qualify for  a  less  stringent   emission limitation  for
 another source  in the same area. In either case,  NOX
 control technologies as efficient as  those required by
 NSPS regulations will be required.
Furthermore, state and local air pollution control agen-
cies may regulate NOX emissions in areas which are in
nonattainment of  the National  Ambient Air  Quality
Standard (NAAQS) or to assure that the standards are
met in the future. For example, some of the air quality
management districts in the State of California are cur-
rently  enforcing  utility and industrial boiler standards
which  are more stringent than the Federal NSPS. In ad-
dition, several  states  — including Texas, Florida, and
New York — are employing an industrial  boiler regula-
tion for existing sources that is equivalent to the propos-
ed industrial boiler  NSPS.
                                             Table 1-4.    New Source Performance Standards for Station-
                                                         ary Gas Turbines"
                                                       Type Turbine
                                  Allowable Emissions
                              Vol. % NOX @ 15% O2, Dry6
                                             Electric utility units with a heat
                                             input at peak load of > 107.2 GJ (100
                                             x 10* Btu) per hour
                                             Units with a heat input at peak
                                             load of > 10.7 GJ (10 x 10" Btu) per
                                             hour but < 107.2 GJ (100 x 10' Btu)
                                             per hour, and units with a base load
                                             at ISO conditions of 30 MW or lessc
                                 0.0075 14.4  + F  (1)
                                 0.0150 14.4  + F  (2)
                                             "Source: 40 CFR, Part 60, Subpart GG. Refer to the source for several
                                             exceptions to the standard.
                                             6Y  = manufacturer's rated heat rate at manufacturer's rated load
                                             (equation 1) or rated peak load (equation 2) in KJ per watt hour, or ac-
                                             tual measured  heat rate based on lower heating value of fuel as
                                             measured at actual peak load for the facility. Y must be no greater
                                             than 14.4. F varies with fuel nitrogen content (by weight) as follows:
                                             for N< 0.015, F = 0; 0.015 < N < 0.1, F = 0.04 (N); 0.1  0.25, F =  0.005.
                                             CISO conditions: 288°K, 60% relative humidity, and  101.3  kPa
                                             pressure.
                                              With this brief introduction as a background, the re-
                                              mainder  of Chapter 1 presents several general topics
                                              designed to establish a background for later sections.
                                              First,  the mechanisms of  NOX formation  are briefly
                                              reviewed. Understanding these mechanisms is essential
                                              to gaining a  full appreciation  for the development of
                                              NOX control technologies, most of which are  aimed at
                                              preventing NOX formation during combustion. Many of
                                              the technologies thus  developed  are  designed  to
                                              primarily  reduce  NOX formation from  the  specific
                                              mechanism associated with a particular combination of
                                              fuel and combustion conditions.
                                              Next, the general schemes for  NOX control are discuss-
                                              ed. An overview is presented of the three classes of
                                              control; that  is, control before, during, and after com-
                                              bustion.  As explained later, control for major sources,
                                              such as coal-fired utility boilers, is limited by practical
                                              considerations and  often  confined to  during-
                                              combustion  technologies.  This is  because  before-
                                              combustion techniques may be unavailable or limited,
                                              and after-combustion techniques may be cumbersome
                                              and cost-ineffective unless also required for control of
                                              other pollutants.

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 Finally,  a subsection  is devoted to  describing the
 sources covered in this manual, namely, utility boilers,
 industrial boilers, gas turbines, and stationary engines.
 This information may be helpful to at least three groups
 of readers: (1) field personnel or managers interested in
 following NOX control developments for other sources
 to ascertain if technologies  can eventually be transfer-
 red to their source; (2) state and local agency personnel
 who may not be totally familiar with the sources that are
 being  regulated; and (3) consultants and  equipment
 vendors who supply engineering solutions to the prob-
 lems of NOX control.  Therefore, the brief discussion  of
 sources is provided for those readers who may feel that
 this background will be necessary to their understand-
 ing  of control  technology applications and results
 presented in later sections.
 1.3   Mechanisms of NOX Formation
 In stationary source combustion approximately 95 per-
 cent of the NOX formed is nitric oxide (NO), which can
 oxidize in the atmosphere to form  nitrogen  dioxide
 (N02), a criteria pollutant. The formation of NOX during
 combustion of fossil fuels occurs by two mechanisms:
 oxidation of atmospheric nitrogen present in the  com-
 bustion air at elevated temperatures (usually called ther-
 mal NOX), and oxidation of a  portion of the bound
 nitrogen in the fuel (fuel NOX). The latter is less depen-
 dent on temperature than on fuel nitrogen content, fuel
 properties, and the stoichiometric conditions present at
 combustion.  The two  mechanisms  are  shown
 schematically in  Figure 1-1.  In  general, fuel  NOX is
 responsible for the bulk of NOX formation in the  com-
 bustion of coal and certain fuel oils with high nitrogen
 content.  For combustion of gas or low nitrogen fuel
 oils, thermal NOX is the dominant mechanism.

 Two important reactions in thermal NOX formation are:
         Figure 1-1.   Basic Mechanism of NOX Formation.
 N2 + 0 = NO + N
N + 02 = NO + 0
(1-1)
(1-2)
Note that  Reaction  1-1, which  is highly temperature
dependent, provides the atomic nitrogen (N) necessary
for Reaction  1-2. Both reactions, however, are equally
important in terms of the amount of NO formed. Note
further that the reverse reactions are not favored by the
presence of molecular oxygen; therefore, in the oxidiz-
ing  environment that normally prevails  downstream
from the actual combustion (due to excess air for com-
bustion), the  NO that has been formed is essentially fix-
ed. Finally, it  has been noted that in regions of the com-
bustion chamber in which the temperature is less than
1,200C (2,200F), formation of NO is not significant.

The kinetics  of fuel  NOX formation are not as well
understood as thermal NOX. The most significant fac-
tors in fuel NOX formation are nitrogen  content of the
                              High Temperature
                                Combustion
                                  Process
        fuel and the degree to which the fuel is mixed with air
        during  the  early stages of combustion when bound
        nitrogen is liberated from the fuel. Table 1-5 shows the
        nitrogen content of selected fuels, including  several
        nontraditional fuels, some of which exhibit relatively
        high  nitrogen  contents.  The  molecular nitrogen in
        natural  gas responds in the same way as nitrogen in the
        combustion air. Because it is  not bound it does not
        behave as fuel nitrogen.

        Table 1-5.    Typical Nitrogen Content of Selected Fuels
                                                                          Fuel
                                               Nitrogen
                                               Content,
                                              Weight %
Coal, anthracite, Pennsylvania          0.6-1.4
Coal, high-volatile "B," Ohio            1.4
Coal, subbituminous "B," Wyoming       1.0
Lignite, North Dakota                  1.7
Fuel oil, No.  1                       0.003
Fuel oil, No. 2                       0.006
Fuel oil. No. 4                       0.24
Fuel oil. No. 6, low sulfur             0.28-0.5
Tar sands oil                        0.07
Shale oil                           0.01
Coal-derived synthetic oil
  SRC-II heavy distillate               1.03
  H-Coal                           0.57
Natural gas, mid-continent              3.2*
Natural gas, Pennsylvania              1.1*
Coke oven gas                       3.4
Crude oil
  Kern Co., California                 0.5-0.83
  Saudi Arabia, light	0.098

*Molecular nitrogen, N2.

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As the fuel enters the flame zone, it is pyrolyzed into
small,  reactive, nitrogen-containing  molecules which
react with oxygen to form NO. If little oxygen is present,
as in the fuel-rich zone of staged combustion  (a com-
bustion modification  NOX reduction technology),  the
nitrogen-containing fuel fragments encounter and react
with each other, and convert the nitrogen to molecular
nitrogen (N2).

This theory then serves as  the basis for many of  the
combustion modification technologies  for NOX reduc-
tion that are discussed in this document.
1.4   General Schemes for NOX Reduction
Because NOX formation results primarily from combus-
tion, three general schemes for NOX reduction suggest
themselves immediately:

•  Reduction before combustion by reducing potential
   for formation
•  Reduction during combustion by modification of the
   combustion process itself
•  Reduction after combustion by some means of flue
   gas treatment.

These are shown schematically in Figure 1-2; the con-
trol technologies shown are described in detail later.

Precombustion schemes for reducing NOX  center on
switching to  fuels with a lower nitrogen content or  a
lower flame  temperature. The choices are severely
limited, however. The fuel choice is usually dictated by
economic factors that transcend the economics of NOX
control. Furthermore, because nitrogen in solid and li-
quid fuels is chemically bound to organic chemical con-
stituents, it is not  efficiently  removed. Therefore, no
technology similar to physical cleaning of coal for sulfur
removal is practical.
Emulsifying diesel oil with water is essentially a combus-
tion  modification technique in that the emulsification
itself lowers the flame temperature and aids atomiza-
tion. However, because it involves pretreatment of fuel,
this technology is discussed further in Chapter 2  under
precombustion control technologies.
NOX reduction during combustion, usually referred to
simply as combustion modification, has been employed
since the early 1970s to effect moderate NOX emission
reductions. It is currently the principal NOX reduction
scheme  for  moderate  control;  a  growing list  of
technologies in this category is being studied or applied.
These technologies,  discussed in detail in Chapter 2,
suppress thermal or fuel NOX by modifying the condi-
tions  for  combustion,   namely,  stoichiornetry,
temperature, and residence time. These modifications
can  be achieved by modification  of the burner itself or
externally through modification of the air or fuel flow to
the  combustion chamber. Research, as well as pilot-
scale and full-scale development of these technologies,
is being carried out primarily by burner and boiler manu-
facturers, the Environmental Protection Agency (EPA),
the Electric Power Research Institute (EPRI),  and the
Gas Research Institute (GRI).

Postcombustion schemes all involve some type of treat-
ment of the flue gas and are normally classified as dry or
wet processes. Some — mostly wet processes — are
also designed for simultaneous removal of sulfur diox-
ide, primarily from coal-fired boilers. Many of the flue
gas treatment processes have been developed in Japan,
where NOX emission limits  are generally stricter than in
the United  States and where  sulfur oxides  (SOX)
removal processes have been widely applied.

Dry flue gas treatment processes usually consist of
either reduction of  NOX to  nitrogen by reducing agents
or adsorption onto solids. The reduction processes may
be' catalytic or noncatalytic.  Noncatalytic reduction is
typified by the Exxon Thermal DeNOx process in which
ammonia   is used  to  selectively reduce  NOX  at
temperatures of 925 to 980C (1,700 to 1,800F) and by
the EPRI urea injection process. These reduction pro-
cesses may emit residual  reducing agents (principally
ammonia) and their  by-products such  as ammonium
sulfate. Adsorption processes add expense due to the
solid waste generated.
Wet  flue gas treatment processes offer perhaps only
one advantage over dry  processes —  simultaneous
removal of sulfur oxides. These processes may be at-
tractive  for applications requiring  stringent  control of
both pollutants. These processes  are currently in the
development stage and have not been commercially ap-
plied in the United States.
Figure 1-2.   General Schemes for NOX Reduction.
     PRECOMBUSTION TECHNIQUES
     •  Switch Fuel
     •  Emulsify Fuel with Water
     •  Fuel Denitrification
     COMBUSTION MODIFICATION TECHNIQUES
     •  Stoichiornetry
     •  Temperature
     •  Residence Time
     FUEL
                 Combustion
                   Chamber
                               EXHAUST
                              OR FLUE GAS
     POSTCOMBUSTION TECHNIQUES

     • Flue Gas Treatment, NOX Only
     • Simultaneous SOx/NOx Treatment
                         4

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 To summarize, although there are a myriad of theoreti-
 cal options currently available for reducing NOX emis-
 sions from combustion sources, the actual selection for
 a specific case will come down to a few very practical
 choices. Until a few years ago nearly all NOX reduction
 for stationary sources was brought about by  simple
 combustion modification.  Recently, however, catalytic
 postcombustion technologies  have  been employed in
 increasing numbers, particularly for stationary engines.

 The normal sequence has usually been to reduce NOX
 emissions from stationary sources with the simplest and
 most economical  combustion modification that will
 achieve the necessary emission  reduction. As further
 reduction is required, progressively more efficient (and
 more difficult to implement  and hence  more costly)
 combustion modifications are employed.  In the case
 where the most efficient combustion modification still
 does not bring about the required reduction, postcom-
 bustion technologies are considered, often in addition
 to one or more combustion modifications.

 1.5  NOX Emission Sources Considered in
 This Document
 This  document considers  the  following stationary
 sources of NOX emissions:

 •  Utility boilers, which account for approximately 53
   percent of all stationary source emissions
 •  Industrial boilers, accounting for about 14 percent
 •  Gas turbines and stationary engines (gas and diesel),
   which together  represent approximately 22 percent
   of stationary source emissions.

 Therefore, this document covers technologies that ap-
 ply to about 90 percent of the stationary sources of NOX
 emissions. Not covered in this document  are commer-
 cial boilers, residential heaters, enhanced  oil recovery
 steam generators, industrial process  heaters,  and
 miscellaneous combustion and noncombustion sources
 which account for  most of the remaining 10 percent of
 emissions.
 Each major source will now be described in detail suffi-
 cient to  provide the  necessary  background for
 understanding  the later discussions   of  control
 alternatives.
 7.5.7  Utility Boilers
 Approximately 80 percent of fossil fuel steam genera-
 tion is from coal firing.(2) The remainder is nearly evenly
 divided  between  natural gas  and  oil  (predominantly
 residual fuel oil such as No. 6). In addition, the uncon-
 trolled NOX emission factors for coal-fired boilers are
 approximately twice those for natural gas-fired and oil-
 fired units (on a Btu basis).

 All  fossil  fuel-fired utility boilers generate steam  by
transferring the heat from  combustion of the fuel to
water. The steam, in turn, produces electricity by ex-
panding through a turbine. The steam generated may
be saturated or superheated and is essentially always
confined inside the tubes with the outside of the tubes
exposed in part to combustion gases. This is the water-
tube arrangement as opposed to the fire-tube arrange-
ment found in low capacity industrial boilers.

Coal is fired either in a bed, or stoker, or in  a state of
suspension. Stoker-fired units are rarely found in large
utility boilers and in terms of nationwide NOX emissions
are of  much  less  importance than  suspension-fired
boilers.

Suspension-fired boilers are categorized (Figure 1-3) as
either cyclone-fired or  pulverized  coal- (PC)  fired
boilers.  Cyclone boilers fire  coal ground to about a
4-mesh  size and carried into a cylindrical combustion
chamber by primary air in a cyclonic flow pattern. Small
particles  burn   in suspension  while larger  particles
adhere to the  molten slag on the furnace walls where
they are burned with the addition of secondary combus-
tion air.

In contrast, pulverized coal-fired boilers fire coal of par-
ticle sizes on the order of 70 percent  passing 200-mesh.
The coal particles burn in a state of suspension in  the
combustion chamber.

For our purposes, these boilers are categorized in accor-
dance with the position  of the burners in the combus-
tion chamber  (Figure  1-4).  Wall-fired  boilers  have
burners mounted  horizontally either  in a single  wall
(front or rear) or in two opposite walls horizontally  op-
posed.  Turbo-fired boilers  also  employ burners in
horizontally opposed pairs but the burners are inclined
downward to  induce a turbulent flow.  Tangential- or
corner-fired boilers employ burners  in groups of  four,
each firing horizontally from a corner of the furnace. At
each elevation of four burners, each burner is aimed at
the tangent to an imaginary circle in the center of  the
furnace,  which  sets up a vertically oriented vortex
throughout the combustion zone. Arch- or vertical-fired
boilers employ burners that fire vertically downward in-
to the combustion chamber and may exhibit a turbulent
flow pattern if the horizontally  entering secondary air
flows are so designed. This type of  boiler is effectively
obsolete but may find application again in the future for
combustion of difficult-to-ignite fuels, such as chars
from  coal conversion  processes, which are low in
volatile matter.

The method of  ash removal is  also important to NOX
emissions in suspension-fired boilers  and is another way
to classify such  boilers.  Dry-bottom boilers burn coal
with a high ash  fusion temperature and therefore  are
designed for a dry ash removal system. On  the other
hand, wet-bottom, or slag-tap,  boilers remove molten
ash (slag) resulting from  combustion of coal with lower
ash fusion temperatures. Wet-bottom boilers exhibit
higher uncontrolled NOX emission rates than do dry-
bottom boilers due to higher combustion temperatures.
Combustion in these boilers  is very intense; thermal
NOX formation is increased  by the higher temperature
while fuel NOX formation is enhanced by the more tur-
bulent mixing.

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Figure 1-3.    Classification of Coal-Fired Boilers.
Figure 1-4.
            Utility Boiler Firing Configurations for
            Pulverized Coal .
          Wall-Fired,
        Elevation View
                                Horizontally Opposed,
                              Wall-Fired, Elevation View
                      Turbo-Fired,
                      Elevation View
        Arch-Fired,
       Elevation View
                                 Tangential Firing,
                                    Plan View
Stoker-type  boilers  are classified  according  to  the
method of feeding coal shown in Figure 1-5.

The four main  burner configurations in coal firing  —
wall-fired  (single),  horizontally opposed-fired,  turbo-
fired, and tangential-fired — also predominate for oil-
and gas-fired  utility  boilers,  although  the   burners
themselves are different.

The most frequently used burners for oil or gas combus-
tion are  the  circular burner and the cell burner. These
burners are also used for pulverized coal or for firing any
of  these fuels  in  combination.  The  maximum firing
capacity of the individual circular burner is on the order
of 165 million Btu/h; cell burners can fire up to about
495 million Btu/h.

The chief difference between the two types of burners
is the fuel injection location. In  the circular burner, fuel
is introduced at one location — the center of the circle.
In the cell burner, fuel  is introduced through multiple
spuds  arranged  annularly around the center  of the
burner. Each spud is a pipe with a pattern of  holes at the
end to discharge the fuel. Figure 1-6 depicts a  circular
burner and Figure 1-7 shows a cell burner. (4)

Figure 1-8 shows a "typical" utility boiler —  in this case
a pulverized  coal-fired boiler employing horizontally op-
posed burners.

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Figure 1-5.   Main Types of Stokers Used in Industrial
            Boilers (3).
 Figure 1-6.    Front View of Circular Burner Used for Oil
             Combustion.
 (a) Underfeed
        .vy» •.••'•'.• Fuej .';•;•:'r:V
               i _ i _ :: _ — -/,/
                    i ________ *
                    Air
                                  Ash Pit
  (b) Crossfeed Spreader
   crc*
             *V            I           « i_ i-t'^
                         Air
                                     Ash Pit
                                                          Impeller
                                                                                               Oil Atomizer
                                               Residue    Figure 1-7.   Front View of Cell Burner Used for Gas
                                                                    Combustion.
                                                        Gas Spud
                                      Impeller
  (c) Overfeed Spreader
7.5,2  Industrial Boilers
Industrial boilers, used primarily to generate steam for
heating or process uses, also fire coal, oil, gas, or waste
fuels. Most coal-fired industrial boilers are water-tube
boilers; fire-tube boilers  are subject to ash plugs and
other  operational  problems.   Large  coal-fired  units
(steam  flow rate greater than 350,000 Ib/h) generally
fire pulverized coal and are very similar to comparably
sized utility boilers. Smaller coal-fired  industrial boilers
(less than  100,000 Ib/h of steam) are normally stoker
fired, and a mixture is found in the middle size range.
Because of the  vast number of smaller boilers, stoker
firing accounts for most of the coal consumption by in-
dustrial boilers.

The main stoker  types in use are illustrated in Figure 1-5.
Spreader stokers propel  coal  into  the  combustion
chamber; a portion of the coal actually burns in suspen-
sion while the remainder burns on a grate. Grates may
be  of the stationary,  dumping,  or travelling  variety.
Because they do not allow for continuous removal of
ash,  stationary grates must be  zoned  to allow for
periodic removal. That is, not all zones are firing at any
one time; this  allows ash removal from one zone at a
time. The underfeed stoker employs a ram to feed coal
upward through the burning bed in the same direction
as the flow of  combustion air to the tuyeres. Multiple
retort underfeed stokers are used for coking coals with
high ash fusion temperatures. In contrast, the overfeed
stoker supplies coal to the bed from above. The latter is
normally used with travelling or pulsating grates and is
amenable to burning nearly all types of coal.

Oil- and gas-fired industrial boilers are either water-tube
or fire-tube boilers. The former employ burner flames on
the  outside of the tubes with  boiler water  flowing
through the tubes,  while the latter reverse this design.
Fire-tube boilers tend most often to be small, packaged
units, whereas  water-tube boilers can be either packag-
ed units or large, field-erected units. Packaged units are
available up to  a capacity of 350,000 Ib/h of steam.

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Figure 1-8.   Pulverized Coal-Fired Boiler Employing
           Horizontally Opposed Burners (5) •
      To
   Precipitator
        Burners

        Underfire
        Air Ports
                                          Burners
                                          Underfire
                                          Air Ports
1.5.3  Gas Turbines
Gas turbines are used in industry for compressing gas or
pumping liquids, and in utilities for generating electric
power. Gas turbines fire natural gas or fuel oil; the oil is
normally a distillate such as No. 2 fuel oil. The principle
of operation is simply to expand the  products of com-
bustion through a turbine to generate power.
The combustion chamber of a gas turbine typically con-
sists of two zones: the primary zone, where essentially
all of the combustion takes place under low  excess air
conditions; and the secondary zone,  where secondary
air is introduced in quantity sufficient to cool the pro-
ducts of combustion to a temperature compatible with
the turbine materials of construction.

There  are  basically three  configurations for gas tur-
bines.  The so-called simple-cycle turbine is the basic
type of gas turbine (Figure 1-9). Compressed air and
fuel  are directed to the combustion chamber, where
combustion and dilution of exhaust gas take place. The
exhaust gas is then expanded through the turbine which
provides energy not only for the load (pump, generator,
etc.) but also for the combustion air compressor.

The  first refinement of the simple-cycle turbine is the
regenerative-cycle  turbine.  This engine uses a simple-
cycle turbine but also includes a recuperative heat ex-
changer to preheat combustion air with the turbine ex-
haust gas. This engine is more energy-efficient than the
simple-cycle gas turbine.

The second refinement is the combined-cycle turbine.
The heart of this type of turbine is a simple-cycle tur-
bine, but it also includes a waste heat boiler to produce
steam  from heat exchange  with  the turbine exhaust
gas.

1.5.4  Stationary Reciprocating Engines
This  category of  NOX emission  sources  includes
compression-ignition   engines  and  spark-ignition
engines (see Table 1-6). Compression-ignition engines
are normally fired with diesel oil or with a combination
of oil and natural gas (generally the oil is injected into
the cylinder only to initiate combustion). The latter are
referred to as dual-fuel engines. Spark-ignition engines
are  typically  fired  with  natural   gas.  Stationary
reciprocating engines have wide-ranging uses; perhaps
their  most important application, involving  units of
several thousand horsepower,  is  to  drive large com-
pressors in distribution of natural gas.

Compression-ignition engines are normally four-cycle
engines of large bore that operate on this familiar cycle:
admission of air and fuel;  compression and  ignition;
expansion;  and exhaust.  Thermodynamically,  com-
pression-ignition engines follow  a constant pressure, or
diesel, cycle. Compression ratios are relatively high (on
the order of 20 to 1) and compression pressures range
up to several hundred psi. At such  high pressures, com-
bustion is spontaneous; therefore, no ignition sources
(such as sparkplugs)  are required.
Spark-ignition  engines  follow  the   spark-ignition,  or
Otto,  cycle of  constant volume combustion.  These
engines feature either four-cycle  or two-cycle  opera-
tion. In two-cycle operation, the air-fuel mixture is com-
pressed outside the cylinder and expels  the exhaust
upon entering the  cylinder.  In two-cycle engines,  a
scavenging arrangement is normally used in order  to
hasten  the exhaust of  combustion products  and
minimize the escape of the air-fuel mixture with the ex-
haust. Immediately after the bulk of the  exhaust gas
leaves the cylinder,  a jet of scavenger air enters the
cylinder.  The  scavenger air  is deflected  usually into
either a helical or cyclic pattern in  order to force the re-
maining exhaust gas out the exhaust port.  The cylinder
is then relatively exhaust-free when the air-fuel mixture
is introduced,  which occurs nearly simultaneously with
scavenging. The pressure for scavenging  can be sup-
plied by the crankcase (common in smaller engines)  or
by an external  blower that is driven by the engine (com-
mon in larger engines).
1.6   Organization of This Document
The remaining chapters are devoted to a more in-depth
examination of NOX control technologies, specifically as
they apply to, and have been refined for, the sources of
NOX discussed earlier in this chapter.
                         8

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figure 1-9.    Simple-Cycle Turbine.
       AIR
                                              Combustion
                                                Chamber
                                            A
       Shaft
                                                                                      Turbine
                             External
                             Load
 Table 1-6.    Characteristics of Stationary Reciprocating Engines

                                               Spark-Ignition
                                    Compression-Ignition
            Typical fuel

            Thermodynamic cycle
            Compression ratio
            Maximum cylinder pressure
            Operation
            Scavenging
Natural gas

Otto (constant volume)
6:1 to 12:1
Over 2,000 kPa
2-cycle or 4-cycle
Usually required for 2-cycle;
crankcase pressure or
external blower used
Diesel oil or dual fuel (oil and
natural gas)
Diesel (constant pressure)
11.5:1 to 22:1
Over 4,800 kPa
Usually 4-cycle
Not required for 4-cycle; 2-cycle
engines often employ blower-
scavenger
Chapter 2 presents a detailed discussion of all the NOX
control  alternatives  that  are  generally  commercially
available and for which performance or cost data are
available.  Most pilot-plant technologies and  untested
conceptual designs are not included here; rather, those
technologies offering a reasonable promise for success
are presented. Chapters 3 through 5 present actual NOX
reduction data  and system cost data for application of
these technologies to utility and large industrial boilers,
                 packaged boilers firing oil or gas, gas turbines, and sta-
                 tionary reciprocating engines. Both retrofit and new ap-
                 plications are considered where quality data on each are
                 available. Note that no  new cost data were developed
                 for this document;  rather, cost data appearing in the
                 literature are merely reported as they were found in the
                 references. Therefore, this report makes no representa-
                 tion as to the accuracy of such cost data.

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                                              Chapter 2
                                     NOX Control Alternatives
2.1   Introduction
Three conceptual schemes for reducing NOX emissions
from stationary sources of combustion were introduced
earlier: precombustion, or the reduction of potential
formation; combustion  modification; and postcombus-
tion removal of NOX from the flue gas. The numerous
technologies that are commercially available for NOX
reduction are now described in some detail, grouped in-
to the above three categories. A more complete discus-
sion of these technologies including results achievable,
associated costs, and deleterious impacts, is presented
in Chapters 3 through 5.
2.2   Precombustion Control
Technologies
Switching to a lower nitrogen fuel is often economically
unattractive, and removal of fuel nitrogen is usually not
cost-effective solely for NOX control. Furthermore, with
many fuels such as natural gas and low-nitrogen fuel oil,
the majority of NOX emissions are from thermal NOX
formation. Therefore, the choices  in this category are
quite limited.  The process of removing sulfur from fuel
oil by  hydrodesulfurization  has the  side  benefit  of
nitrogen removal but is very expensive in  comparison
with combustion modification techniques that produce
a comparable NOX reduction.

2.2.1   Change of Fuel
Clearly, this is the trivial case. Where it is economically
attractive to change to a lower nitrogen fuel, changes
for economic  reasons, not for NOX reduction incentives,
have been or are made.  Cost considerations are para-
mount and merely switching to a  lower nitrogen fuel
may not effect a large enough  reduction to meet NOX
emission  regulations,  which  in  any case  are  fuel-
specific.  Therefore, combustion  or  postcombustion
NOX reduction techniques may be necessary.

2.2.2   Fuel Oil/ Water Emulsions
This control technology could arguably be classified as
a combustion modification technique because it alters
the conditions for combustion; however, it is discussed
here because  it involves mixing of fuel prior to combus-
tion. The  technique has  been tested  on stationary
engines firing diesel fuel. Tests of this technique have
been typically performed on diesel engines in the 100 to
300 hp size range and have employed fuel mixtures from
7 to 45 percent water. Emulsions have been  delivered to
the fuel injection system in a number of ways: a simple
mixer and pump arrangement; a low-energy shear fluid
mixer into which the oil-water mixture is pumped; or a
high-energy emulsor in which the mixture is pumped
through an orifice at a high (on the order of 2,000 psi)
pressure drop.

The primary mechanism for NOX reduction provided by
fuel oil/water  emulsions  is  lowering  of the flame
temperature. Heat transfer from the flame to the flue
gas is enhanced by the presence of water vapor which
serves to increase the overall specific heat capacity of
the products of combustion, thus lowering  the flame
temperature. Another probable mechanism taking place
is the  limiting of the NO formation reaction resulting
from the water vapor's dilution of the oxygen in the
flame zone. Finally, the rapid vaporization of water in an
oil droplet is thought to increase the atomization of fuel,
thus enhancing combustion efficiency.


2.3   Combustion Modification
Technologies
The majority of NOX control technologies for combus-
tion sources involve modifying the  parameters of com-
bustion. All  of the techniques are  aimed at  achieving
one  or more  of the following goals: reducing the
available oxygen at critical stages of combustion; lower-
ing the peak  flame temperature;  and reducing the
residence time during which oxidation of nitrogen takes
place. Table 2-1 summarizes the technologies covered
in this subsection and  the  mechanisms  these
technologies rely on.

Where possible, the technologies to be considered
under this heading  have been grouped by similarity and
ordered by degree of complexity. Retrofit technologies
are presented first, in order of increasing complexity,
followed by technologies for new combustion sources.

In terms of  meeting compliance NOX emissions levels
both on a source-by-source basis and in a general sense
for fossil fuel-fired boilers as a whole, a logical progres-
sion of control technologies can be employed in order of
increasing removal  efficiency and cost. In this manner
the appropriate and most cost-effective technology can
be found most expediently.  For example, low excess air
would  be  the  first technology  employed; if the NOX
emission reduction achieved at the limit of low excess
air is not sufficient, any of various types of staged com-
                                                 11

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Table 2-1.    Combustion Modification Technologies
Technology
Low excess air
Staged combustion
Lowers Flame
Temperature
Yes
Reduces
Available
Oxygen
Yes
Yes
Shortens
Residence
Time
-
Other
-
            BOOS
            Biased firing
            Overfire air
            Arch firing
          Reducing combustion air
            preheat
          Water injection
          Exhaust gas recirculation
          Low NOX burners
            Staged air
            Staged fuel
            Variations
          In-furnace destruction
            (reburning)
          Lean-burn, torch ignition
          Turbocharging
          Charge cooling
            (refrigeration)
          Retardation (ignition
            or injection)
Yes

Yes
Yes
Yes
Yes
Yes
Yes

Yes
Yes
                 Yes
                          Reduction
                         of NO to N2
               Yes
bustion typically would be applied. The logical progres-
sion would  proceed in this manner until the desired
reduction is achieved.  As mentioned earlier, this pro-
gression applies for individual sources and also parallels
the development of these technologies to  meet ever-
increasingly stringent NOX emission levels.  For retrofit
applications, the feasibility and cost effectiveness are
dependent on space requirements and operational side
effects resulting from modified combustion  conditions.
Some  control technologies may  not be practiced
because  of  cost or effect on boiler  efficiency.  In any
event,  the actual order in which  technologies are im-
plemented depends on  the required emission reduction.

2.3.1  Low Excess Air
Operating burners with low excess air is perhaps the
simplest  NOX reduction technology to implement on a
retrofit basis; no capital equipment is required and com-
bustion  chamber  modifications are  normally  un-
necessary. However, the NOX reductions achievable are
modest and may not,  in specific  retrofit situations,  be
sufficient to comply with NOX emission regulations. The
degree of control is constrained by the onset of carbon
monoxide (CO) emissions (generally  held to 50 to 100
ppm) or plume opacity at low excess air. Other factors
such as safety considerations (e.g.,  minimum air flow
requirements) may also be considered. The  technology
is applicable to coal, oil, and gas firing in boilers of all
sizes.

Most new coal-fired boilers are designed for low excess
air firing. In order to  meet  New  Source Performance
Standards,  however,  they also usually are equipped
                 with low NOX burners or other combustion modification
                 NO* reduction technique. Oil-fired and gas-fired boilers
                 in many instances can be operated at excess air levels of
                 5 percent  and lower.  However, coal-fired boilers nor-
                 mally require a greater excess air level in order to ensure
                 essentially complete carbon burnout and  to  minimize
                 emissions of carbon monoxide.

                 The low excess air method accomplishes NOX reduction
                 of both thermal and fuel NOX. Reduced availability of
                 oxygen suppresses the formation  of NO from nitrogen
                 in the fuel and in the combustion air.

                 2.3.2   Staged Combust/on
                 Staged combustion is actually  a  whole family  of
                 technologies. The most frequently employed for retrofit
                 of large industrial and utility boilers are burners out of
                 service (BOOS) and biased firing.  For new units, over-
                 fire air is most frequently applied. Arch firing, a boiler
                 configuration inherently low in NOX formation, has also
                 received attention lately as a form of staged  combus-
                 tion. Staged combustion can also be achieved internally
                 by burner modification.  A  key  characteristic of this
                 technology is stretching of the combustion zone, which
                 may cause   flame  impingement on  side  walls  or
                 superheater tubes and affect steam balance and conse-
                 quently  unit  efficiency.  When  staging  lowers
                 stoichiometric air ratios below 1.0, there is the potential
                 for increased  tubewall corrosion rates.

                 2.3.2.1  Burners Out  of Service (BOOS)
                 This technology is generally applicable to wall-fired utili-
                 ty and large  industrial boilers.  BOOS  is normally im-
                        12

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plemented on existing units by employing an upper row
of burners — on one wall or on both walls of opposed-
fired units — as sources of secondary combustion air
only,  without  introduction of  fuel  through these
burners. Also, selected burners can be removed from
service other than the top row if  the BOOS pattern is
balanced. The effect is to provide so-called overfire air
above the active burners which comprise the primary
combustion  zone. This zone is maintained under fuel-
rich conditions by introducing  air to these burners at
lower than stoichiometric rates.

Operation of the lower furnace zone with a substoichio-
metric amount of air (fuel-rich conditions) lowers the
conversion of fuel nitrogen  to  nitrogen oxide. Subse-
quent  cooling and dilution of the  combustion gas with
the  secondary air from the  upper (out  of  service)
burners  reduces peak flame  temperature and thus
minimizes the formation of NO by thermal fixation.

BOOS could presumably be employed  in new installa-
tions but finds the vast majority of its applications as a
retrofit technology. It is applicable to suspension-fired
coal boilers as well as boilers firing oil or gas.

2.3.2.2  Biased Firing
Biased firing is a retrofit technology generally only  ap-
plicable to oil-fired and gas-fired utility  and large in-
dustrial boilers. It is roughly equal to BOOS in ease of
implementation;  no  new equipment  is  usually
necessary, nor are any major boiler modifications.

In  biased firing,  the  overall combustion  chamber
stoichiometry is preserved (which  may in all probability
involve low  excess air) while air and fuel flows to in-
dividual burners are varied.  There  is no set or generally
accepted  pattern to variation of the burner conditions,
as many combinations may yield the desired effect. The
goal is to create fuel-rich and fuel-lean regions in the
combustion chamber with  an effect similar to that of
overfire air  or  BOOS: The  fuel-rich regions  generate
relatively low thermal and fuel NOX.  The best combina-
tion is usually found  by experimenting with various
patterns.

2.3.2.3 Overfire Air
The third widely used type of staged combustion  is
overfire air, which is applicable to coal-, oil-, and gas-
fired utility boilers and large industrial boilers. Overfire
air is usually used in new boiler designs. Unlike BOOS
and biased firing, overfire air requires modification of
the combustion chamber. Specifically, air ports above
most or all of the rows of burners must be added to pro-
vide the secondary combustion air above the burners.
The result is similar  to BOOS  operation: Fuel-rich
burners reduce fuel and thermal ISIOX formation, and in-
terstage cooling by boiler tubes  reduces peak flame
temperatures which also suppresses thermal NOX. Over-
fire air operation is shown in Figure 2-1.
Figure 2-1.   Typical Staged Combustion: Overfire Air (6).


                     Furnace Outlet
   Overfire Air •
Main Burner
                   /  COMBUSTION \
                   !  COMPLETION   1
                   v      ZONE     /
 /        \
 '    MAIN   \
/  BURNER   \
. COMBUSTION '
\    ZONE    I
 \        /
2.3.2.4   Arch Firing
This boiler configuration is one of the earliest designs
for burning pulverized coal in utility boilers and is receiv-
ing some attention lately because it is an inherently low
IMOx formation combustion technology. Burners are
mounted such that they fire vertically downward in the
combustion chamber; secondary air is injected farther
down the vertical walls of the boiler. The result is a
J-shaped flame in which the combustion is staged and
therefore NOX  emissions  are  low. Figure 2-2 shows
schematic views of three different arch-fired boilers.

Because this technology involves an entire combustion
chamber configuration, its  applicability on  a retrofit
basis is limited,  especially when  compared to the
relative  ease of retrofitting the furnace  with  low NOX
burners. Its best application may be for new units,
although there are two basic drawbacks:  The cost of an
arch-fired boiler is generally significantly higher than a
comparable wall-fired boiler; and the technology has
not been applied to  new  boiler designs for years and
there may be a natural reluctance on the  part of utilities
to employ it.

2.3.3  Temperature Reduction  Technologies
Several  NO*  reduction technologies  employ  some
method of reducing peak flame temperature to reduce
thermal  NOX formation. These include reducing the
combustion air  preheat,  injecting  water, and  recir-
culating exhaust gas. These technologies are presented
schematically  in  Figure 2-3.  Temperature  reduction
technologies are  generally applicable to oil-  and gas-
fired boilers and  engines; they are  not effective for
sources firing coal or high nitrogen oil because thermal
NOX  formation is usually the less important mechanism
in such units.
                                                                              13

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Figure 2-2.   Arch-Fired Boilers (7).
                                         125 MW
   2.3.3.1  Reducing Combustion Air Preheat
   This technology is applicable primarily to utility and in-
   dustrial  boilers burning  oil or gas.  The technique  is
   merely to lower the temperature of the incoming com-
   bustion air, usually by providing a bypass around the air
   preheater for a portion of the combustion air. The result
   is that the  peak flame temperature is correspondingly
   reduced, thus reducing thermal NOX formation. In utility
   and some large industrial boilers, economizers can be
   used to  recover some of the thermal efficiency that is
   sacrificed  in  reducing  the combustion  air  preheat.
   However, the loss of thermal efficiency can represent a
   severe economic penalty. This technology, therefore, is
   often considered for interim control.

   2.3.3.2  Water Injection
   Water injection technology involves a modest modifica-
   tion to allow water to be injected into the combustion
   air stream.  Normally,  nozzles are mounted in  the wind-
   box in a manner that permits vaporization of  the water
   before it enters the combustion chamber. The vaporiza-
   tion removes some of the  heat from the combustion
   chamber, thus lowering  peak flame temperature.  It is
   important to design the system so that vaporization of
   the water occurs before the combustion air reaches the
   combustion chamber to avoid  corrosion  in this area. As
   it is a temperature reduction technology, water injection
   may also carry a significant energy penalty  and thus
   should perhaps be viewed  as an interim  measure for
   utility boilers.

   2.3.3.3  Exhaust Gas Recirculation
   Exhaust gas recirculation (EGR),  or  flue gas  recircula-
   tion  (FGR), is a technique similar  to  that  used  for
                       275 MW
 Figure 2-3.   Three Temperature Reduction Methods for Boilers
 To Stack
                         Combustion
                             Air
                          Preheater
                                            FLUE GAS
                                                                 flue gas
                                         PREHEATED COMBUSTION AIR
             Bypass a portion
             of eombtisttop air around heater
                             Boiler
                                                     WATER
Inject water
                        14

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automobile engines. In fact its greatest applicability is
with stationary engines and turbines. It is applicable on
a new or retrofit basis for boilers, process heaters, and
engines. A portion of exhaust gas or flue gas is recycled
to a point where it joins, and therefore dilutes, the inlet
combustion air flow. This dilution serves to lower peak
flame temperature,  thus reducing thermal NOX forma-
tion. The local oxygen level in the flame is also reduced,
which helps to suppress NOX formation. This technique
is normally not applicable for coal-fired boilers (where it
is normally called "flue gas recirculation") because the
greater  portion of NOX emissions are from fuel NOX in
coal combustion.
2.3.4  Low NOX Burners
Low  NOX  burners have  been  and  continue  to be
developed for coal-, oil-, and  gas-fired boilers. These
burners are applicable on a new or retrofit basis and can
be  used for  utility boilers, large  industrial boilers, or
small packaged boilers.  Low NOX burners are normally
developed by boiler and burner vendors and therefore
exhibit a wide variety of designs. However, the principle
for  all  NOX  burners is the  same:  They inherently
generate lower NOX emissions due to internal staging of
fuel combustion.

For retrofit of low NOX burners, the number, type and
arrangement  of  original burners, the structural con-
figuration of the firing walls, and the nature of the low
NOX burners to be retrofitted all need to be considered.
Some retrofits are relatively straightforward; however,
others are complex and  may prove to be infeasible due
to the complexity.

2.3.4.1   Staged-Air Burners
One of the  first  low  NOX  burners to  be developed
employs staged air within the burner itself to effect NOX
reductions (Figure 2-4). The effect  is  similar to staged
combustion  except  that  the  detailed design  of  the
burner — as  opposed to the arrangement of burners in
the combustion chamber or the design of the combus-
tion chamber itself — is  responsible for the staged com-
bustion. Low NOX burners of this and other types are
equally applicable in new or  retrofitted boilers. With
some designs, the firebox geometry may not permit a
burner retrofit without derate or flame impingement.

The staged-air burner employs primary and secondary
air for combustion in such a way that conditions in the
primary flame zone are substoichiometric (fuel-rich).
The remaining air (tertiary or staged  air) is injected after
a brief delay  so that the flame experiences a predeter-
mined residence  time under reducing conditions. As
with staged combustion, the peak flame temperature is
thus lowered, resulting in lower rates of NOX formation.

2.3.4.2  Staged-Fuel Burners
In staged-fuel burners,  all  of the air required for com-
bustion is introduced into the primary combustion zone
Figure 2-4.    Low NOX Burner: Staged-Air Design (8).
        Staged
         Air
         Secondary
            Air
Secondary
   Air
                     Primary Air
                      and Coal
(Figure 2-5). The fuel is staged,  however, so that the
amount of fuel which the primary zone receives is less
than stoichiometric. Primary combustion is under fuel-
lean conditions and therefore NOX formation is repress-
ed by the lower flame temperature brought about by the
excess air. The remaining fuel is injected into the flame
through a peripheral pattern of high-velocity nozzles.
Figure 2-5.    Low NOX Burner: Staged-Fuel Design (9).
            Secondary
             Nozzle
Primary
Nozzle
           Secondary
             Nozzle
                                                                             15

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 The design ensures rapid mixing by the entraining ac-
 tion of the injected  fuel,  which brings about results
 similar to exhaust  gas recirculation:  NOX formation is
 reduced by a lower flame temperature in the secondary
 zone and by the decreased availability of oxygen in the
 staged zone.

 2.3.4.3  Variations
 A myriad of commercial variations  of internally staged
 low NOX burners are offered by vendors for both new
 and retrofit applications. For example, Foster Wheeler
 offers the controlled flow/split flame burner for coal-
 fired boilers (Figure 2-6). Adjustable inner and outer air
 registers provide staged air while a tapered annular split-
 coal nozzle separates the coal into several streams and
 thus generates several flames. The result is that primary
 combustion is  at  substoichiometric  (fuel-rich) condi-
 tions and mixing is delayed until the secondary zone.

 Babcock & Wilcox has offered for several years a dual-
 register burner, which is essentially a staged-air burner
 for coal-fired boilers (Figure 2-7). In fact this burner has
 been the standard for all new B&W units sold since
 1972.  Normally, a compartmented  windbox  is also
 employed. Therefore, the company refers to their low
 NOX burner  system as  the  dual-register  burner/
 compartmented-windbox system.

 Riley Stoker offers two major types of low NOX burners
 for coal-fired boilers: the controlled  combustion Venturi
 burner for wall-fired  boilers,  and the directional flame
 burner for turbo-fired boilers. The  former (Figure 2-8)
 provides  a  fuel-rich  zone  along the burner axis sur-
 rounded by layers of progressively leaner mixtures. The
 Figure 2-6.
Low NOX Burner: Foster Wheeler Controlled
Flow/Split Flame Burner (10) •
                     Outer Register
                    for Secondary Air
              Inner Register
            for Secondary Air
   Ignitor
                            Perforated Plate Air Hood
                                       Movable Sleeve
 Flame
Scanner
                                          Split Flame
                                          Coal Nozzle
      Tangential
      Coal Inlet
latter (Figure  2-9)  is actually  a  burner arrangement
wherein the combustion zone is designed to produce
turbofiring and overfire air is used to produce a staged-
combustion effect.

EPA has pioneered the development of the distributed
mixing burner. It consists (Figure 2-10) of a circular
burner that operates under  reducing (fuel-rich) condi-
tions in a  recirculation zone where the inner  secondary
air combines with the primary air and fuel. Tertiary air is
supplied through outer ports. This arrangement allows
sufficient  residence time in the burner zone to  reduce
bound nitrogen compounds to molecular nitrogen and
also allows radiation heat transfer to reduce peak flame
temperatures.  The tertiary air provides an overall oxidiz-
ing atmosphere to efficiently complete the combustion.
These burner concepts can  also be applied with other
commercial  burners.  The use of tertiary  air  ports,
however,  does complicate the retrofit application by re-
quiring modifications to pressure parts.

A type of low  NO* burner — which is actually a burner
arrangement — specifically designed for tangential-fired
boilers  is the low NOX  concentric firing  system
developed by  Combustion Engineering in  conjunction
with EPA. In the conventional tangential-firing arrange-
ment the primary air/fuel and secondary air streams are
aimed at the same imaginary circle in the center of the
combustion chamber. In the concentric firing system
(Figure 2-11),  the secondary air is directed at a larger
concentric circle and therefore the initial  combustion
takes place in an atmosphere of  reduced  oxygen
because the primary air/fuel stream does not entrain
the secondary air stream as rapidly as in the conven-
tional arrangement.

2.3.5  In-Furnace Destruction
This technology, which may be referred to as reburning
or  fuel staging,  is here classified  as a combustion
modification  technique,  although it involves reduction
of NOX after it has been formed in the combustion zone.
The technology is being investigated for both new and
retrofit applications and for utility and large industrial
boilers and for stationary engines, although it has not
yet achieved  full  commercialization in  the  United
States. The technology is applicable for pulverized coal,
gas, or oil.

The principle of in-furnace NOX destruction  by  reburn-
ing  has  been the subject of numerous  investiga-
tions.(13,14,15,16)  Although  the  basic reactions are
similar to those that occur  in staged combustion pro-
cesses,  the   actual pathways  are  rearranged. The
hydrocarbon fragments from the decomposing  reburn-
ing fuel react directly with the nitrogen oxides from the
primary zone to form fixed nitrogen intermediates (e.g.,
HCN), which can  subsequently react under fuel-rich
conditions to  form molecular N2. The  actual extent of
NOX reduction depends on the time and temperature in
the fuel-rich reburning zone. Above the reburning zone,
overfire or burnout air is added to complete the com-
                         16

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Figure 2-7.   Low NOX Burner: Babcock ft Wilcox Dual Register Burner/Compartmented-Windbox System (11).
                                     Compartmented
                                        Windbox
                Typical
                Burner
                      Secondary Air
 Nozzle
  Coal and
 Primary Air
                      Secondary Air
              Section X
                                         Section X
Burner Secondary Air
  Control Dampers
                                                        Burner Secondary
                                                            Air Foils
bustion of unburned material. In this zone, some of the
nitrogen intermediaries can be  reconverted to NO.
Because of this reconversion there is an optimum fuel-
rich stoichiometry that exists for the reburn zone.

Using the reburning concept originated  by Wendt and
Sternling,  Mitsubishi  Heavy Industries  (Japan)
developed  the  Mitsubishi Advanced  Combustion
Technology, or MACT, process (Figure 2-12). The pro-
cess has been tested on various fuels and under condi-
tions where the hydrocarbons for upper injection are the
Figure 2-8.   Low NOX Burner: Riley Stoker Controlled
           Combustion Venturi Burner (5).
               same as or different from the main boiler fuel. Since
               1980 further advances have been made through EPA-
               funded extramural and in-house projects.(17,18,19,20)
               The process can be optimized by using low NOX burners
               in the primary combustion zone  (e.g.,  the low NOX
               pollution minimum [PM] burners shown in Figure 2-12'

               2.3.6  Other Types of Combustion Modifications
               A  significant  number  of  additional  combustion
               modifications are employed for reducing NOX emissions
               from specific sources. Most are employed for stationary
               engines or for turbines. Several of these are considered
               in this section and are shown schematically in Figure
               2-13.
                                       4-Bladed
                                       Conical
                                        Coal
                                       Spreader
  Coal and
 Primary Air
        Burner
        Front
        Plate
                         Venturi
                        Nozzle Tip
      Burner
      Throat
2.3.6.1   Lean Burning, Torch Ignition
This technology is applicable  to stationary  spark-
ignition engines burning natural gas. In this technology,
the air-to-fuel ratio is increased to  a level not normally
attainable by the  use of spark ignition.  An  ignition
chamber, rather than sparkplugs,  is used in which  a
burning jet is created  by igniting  a fuel-rich mixture.
This torch provides the ignition for the engine and ex-
tends the lean limit that otherwise  would be  limited by
misfiring, incomplete combustion,  or overworking the
turbocharger. A possible drawback to this technology
appears to be relatively high levels of hydrocarbon emis-
sions; however, development work in this area is ongo-
ing. The  technology can be applied for new engines or
on a retrofit basis; however, the latter could be quite in-
volved  and would also require extensive engineering to
design  and  construct the  most effective  ignition
chamber.
                                                                              17

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Figure 2-9.   Low NOX Burner: Riley Stoker Directional Flame Burner (5).
      Coal and
     Primary Air
                                                 Directional
                                                  Vanes
                                                               Coal
                                                             Spreader"
s
A





\l


A


i
o
1


V





^



^


I/

                                                                                           Section A-A'
2.3.6.2  Turbocharging

Turbocharging, often employed primarily to increase an
engine's available power, is a technology that also can
be used to reduce NOX  emissions  by changing the
fuel/air ratio to a leaner mixture for stationary engines.
Turbocharging involves  passing  the engine exhaust
                                       through a turbine coupled to a compressor.  The com-
                                       pressor  provides higher  pressure combustion air  and
                                       therefore increases the mass of air in the cylinder per
                                       unit fuel.

                                       Turbocharging is normally employed on a retrofit basis.
                                       In cases where air temperature rises significantly due to
 Figure 2-10.   Low NOX Burner: EPA Distributed Mixing Burner (12).
    Cast
 Refractory
    Exit
                           Tertiary Air Port
                         Adjustable     Primary Air
                         Swirl Vanes    and Coal Inlet
  Fixed Vane
Primary Air Swirl
                                             Oil Gun for
                                              Ignition
                                            Secondary
                                             Air Inlets
                                                           Adjustable Outer
                                        Tertiary Air Port     Secondary Register
                                                         for Swirl Generation     Adjustable Inner
                                                                            Secondary Register
                                                                            for Swirl Generation
                                                                                                          Oil Gun
                                                                                Primary Air
                                                                               and Coal Inlet
   Outer         Inner
Secondary Air  Secondary Air
    Inlet          Inlet

A. Development Distributed Mixing Burners (12.5, 50 and 100
   x 10" Btu/h)
                                        B. Full Scale Distributed Mixing Burner (12.5 x 10" Btu/h capacity)
                          18

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Figure 2-11.  Low NOX Burner: Combustion Engineering Low
            NOX Concentric Firing System (6)-


                      Direction of
                        Axis for
                      Coal/Primary
                        Air Flow
                           \
     Burner
   Assembly
Direction of
  Axis for
 Secondary
  Air Flow
      Burner
     Assembly
                                 Burner
                                Assembly
                                Burner
                               Assembly
 compression,  an  intercooler  is  also required. Tur-
 bocharging  is  applicable  to compression-ignition
 (diesel) and spark-ignition (gas) stationary engines.

 2.3.6.3   Charge Cooling
 This technology, often referred to as charge refrigera-
 tion, is employed in diesel as well as spark-ignition sta-
 tionary engines. Charge cooling can be applied on a
 new or retrofit  basis. The  NOX  reduction principle is
 simply to decrease the peak flame temperature by cool-
 ing the air/fuel mixture prior to combustion. Normally,
 a  refrigeration system is arranged as a heat exchanger
 upstream of the intake manifold to cool the combustion
 air. The air temperature reduction is usually on the order
 of 50 to 75F.

 Charge cooling is often employed in conjunction with
 other  NOX  reduction techniques, particularly multiple
Figure 2-12.
 Additional Air
Upper Burner
Overfire Air
In-Furnace Destruction by Mitsubishi Advanced
Combustion Technology (MACT) Process (21).
                               Combustion
                               Completion
                                 Zone
                                  NOX
                               Decomposing
                                  Zone
                                 Main
                              Combustion
                                 Zone
                                             Figure 2-13.  NOX Reduction Options for Stationary Engines.
               AIR

               Turbocharging provides
               high pressure (and there-
               fore greater mass) air,
               permitting lean burning

               Charge cooling lowers
               peak flame temperature by
               cooling the air/fuel mixture
                                              IGNITION

                                              Torch ignition permits lean
                                              burning (spark-ignition
                                              engines only)

                                              Delayed ignition reduces
                                              the mean residence time of
                                              fuel in the cylinder, thus
                                              shortening the high NO*
                                              emission period (spark
                                              ignition engines only)
                                FUEL

                                Delayed fuel injection
                                reduces the mean
                                residence time of fuel in
                                the cylinder, thus shorten-
                                ing the high  NOX emission
                                period (diesel engines only)

                                Charge cooling lowers
                                peak flame temperature by
                                cooling the air/fuel mixture
sparkplug firing, in order to rectify the problem of misfir-
ing that is often  experienced when combustion air  is
cooled to low temperatures.
2.3.6.4  Retardation
NOX emissions from all types of stationary engines can
be reduced by adjustments that retard either the ignition
timing  (spark-ignition  engines) or  the fuel  injection
(diesel engines). This is strictly a retrofit technology and
is normally applied with  greater  frequency  on  high-
compression (diesel) engines and engines that run lean
(such as turbocharged engines). Retarding both ignition
and  injection delay  combustion for an  instant. The
theory is that the first portion of fuel that burns pro-
duces an inordinate amount of NOX because it is expos-
ed to high temperatures the longest, and because it  is
heated by compression, while the balance of the fuel  is
burned.  Therefore,  this  technology  brings  about  a
reduction in NOX formation by  reducing the dwell time
of the fuel in the cylinder.

An added benefit of NOX reduction by  ignition or injec-
tion  retard is an apparent  reduction  in emission of un-
burned  hydrocarbons.  However, there  is  often an
increase in smoke emissions in diesel engines. Further-
more,  cylinder exhaust valves are exposed  to higher
temperatures with this technology and may experience
reduced life.
                                                                                  19

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2.4   Postcombustion Technologies
There are many technologies for reducing NOX once it
has been formed by the combustion process. These do
not compete directly with combustion modifications but
rather are considered only after the easier to implement
and less costly technologies have been exhausted and
even more stringent control is required. Usually referred
to as  flue  gas  treatment  (FGT)  processes,  these
technologies  are  seldom cost-effective for  moderate
NOX reduction  when  compared  to combustion
modifications for several reasons: relatively high initial
cost, high operating cost,  and  possible waste disposal
costs. Accordingly, these technologies are used when
stringent regulations require high NOX reductions. In the
future, flue gas treatment may be the best approach for
removal of NOX and sulfur oxides, and a number of pro-
cesses are under  development to achieve these goals
simultaneously.

FGT processes can be categorized as either dry or wet
and can  be  further divided by the chemical reaction
principles involved in the conversion. Figure 2-14 shows
these processes, organized by type.

2.4,1  Dry Processes
A wide variety of dry processes are either commercially
available or  well along in  research and development.
They range from catalytic and noncatalytic reduction to
adsorption processes and irradiation with electron
beams.  Dry  processes usually involve  less  equipment
and therefore are less costly than wet processes, and
generally also produce less waste to dispose of.

2.4.1.1   Selective Reduction
Selective reduction technologies are either catalytic or
noncatalytic.  In the United States, both methods have
been employed for oil-fired and gas-fired utility  and in-
dustrial  boilers and  process   heaters  and  are being
researched for use in coal-fired utility boilers. In  addi-
tion, catalytic processes have been   used  for spark-
ignition stationary engines and for gas turbines.
In selective catalytic reduction (SCR), which is the most
popular FGT process in international utility use today,
ammonia is employed as the reducing agent. In the SCR
process,  NOX is reduced to  N2 and H20  by  ammonia
(NH3) at 300-450°C in the presence of a catalyst. NH3 is
an acceptable  reducing agent for NOX in  combustion
gases because it selectively reacts with NOX while other
reducing agents, such as H2,  CO, and CH4, readily react
with 02  in the gases. Figure 2-15 shows  a  typical
flowsheet for  a selective catalytic  process  with am-
monia. Flue gas from  the boiler is  passed through a
reactor column which  contains the catalyst  bed.  So-
called parallel flow catalyst beds may be used in which
the gas flows  through channels rather than pores to
minimize blinding  of the catalyst by particulates. Am-
monia vapor is injected into the flue gas upstream of the
reactor. The treated flue gas then passes through the
combustion air preheater and then  to paniculate and
perhaps sulfur dioxide removal equipment before ex-
iting up the stack. The major items of process equip-
ment are the reactor and  the  equipment  to  store,
vaporize, and inject ammonia.
In the early stages of  its development, SCR had the
following  problems: catalyst  poisoning by SOX  in the
gas; plugging  of  the catalyst by  dust;  ammonium
bisulfate deposition on the catalyst below about 300°C;
ammonium bisulfate  deposition in  the air  preheater
below about 250°C; catalytic promotion of oxidation of
SO2 to S03; and erosion of the catalyst by fly ash from
coal. (22)

Those problems have been addressed by the following
countermeasures:

•  Use of base metal  catalysts with  Ti02 instead of
   AI203 or Fe203 substrates
•  Use  of parallel-flow type catalysts  such  as
   honeycomb, plate, and tube catalysts
•  Maintaining the gas temperature above 330°C by us-
   ing an economizer by-pass system
Figure 2-14.  Classification of NOX Flue Gas Treatment Processes .
Blocks may represent several available processes,
and many processes simultaneously remove SOX.
                        20

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Figure 2-15.  Typical Flow Diagram for Selective (Ammonia)
           Catalytic Reduction Process (8).
                                          Figure 2-16.   Thermal DeNOx System — Process Flow
                                                      Diagram (8).
        Boiler
 Coal
i Flue Gas
                                       Flue Gas
                                    Desulfurization
                                        Unit

                                            H\
                                              Stack
    Unloading
    Compressor
 Rail or
 Truck Hook-Up
   Ammonia A Steam
 Storage Tank/
                                                Air
                      NH3 Vaporizer
•  Keeping unreacted NH3 (IMH3 at the reactor outlet)
   below about 3 ppm
•  Using a low-oxidation catalyst
•  Using a moderate gas velocity, a hard catalyst, and a
   device for erosion prevention such as dummy spacer.

There  are  two  noncatalytic  selective reduction pro-
cesses. The Thermal DeNOx process was developed by
Exxon  and is shown schematically in Figure 2-16.  It
employs ammonia as the reductant but the reaction is
carried out at high temperature rather than under the in-
fluence of a catalyst. A similar process  using urea as the
reducing agent was developed by EPRI.I23) Both pro-
cesses  require that the reducing  agent be  injected
directly into the superheater section of the boiler; it is
therefore less complicated and expensive to  retrofit
than the catalytic process. However, temperature con-
trol is critical  to avoid producing more NO or releasing
unreacted reductant to the stack;  therefore, ensuring
that the injection  is at the right  place  even though
temperature patterns fluctuate is difficult and may limit
the reduction efficiency. This  process  is being used for
several boiler  heaters, primarily on the  West Coast.

2.4.1.2   Nonselective Reduction
This  technology  encompasses  catalytic  reduction
without  a  reductant that is selective   to  NO.  This
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                                           technology involves application,  on a new or retrofit
                                           basis, of a catalytic converter of the type employed in
                                           most  newer automobiles in the  United  States.  The
                                           technology in terms of stationary  sources is limited to
                                           stationary reciprocating engines, particularly rich-burn,
                                           spark-ignition engines.

                                           This  technology is applied  by installing the  catalytic
                                           converter in the exhaust line from the engine. The con-
                                           verter consists  of a catalyst  bed supported  within  a
                                           pressure-tight  housing.  Exhaust  gas  passes straight
                                           through with a large percentage of the NO reduced to
                                           molecular  nitrogen.  Catalysts employed are  normally
                                           noble metals such as platinum.

                                           2.4.1.3  Simultaneous NOX/SOX Removal
                                           Dry processes for simultaneous NOX/SOX removal that
                                           are  under  development include  reaction of  sulfur
                                           dioxide (S02)  with  copper  oxide simultaneous with
                                           selective catalytic reduction of NOX with ammonia; ad-
                                           sorption onto  alkalized alumina;  and  irradiation with
                                           electron beams. Although many process concepts are
                                           promising, they have not been demonstrated commer-
                                           cially in the United States.

                                           2.4.2   Wet Processes
                                           Most wet flue gas treatment processes for NOX removal
                                           represent  natural extensions of  processes  originally
                                           developed for SOX  removal only. To date,  wet  pro-
                                           cesses are still in the developmental stage. Thus they
                                           cannot be  considered  as alternatives until  they ex-
                                           perience technical breakthroughs.
                                                                              21

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                                                Chapter 3
                                    Performance and Cost Data:
                                Utility and Large Industrial Boilers
3.1    Introduction
In this chapter data on  NOX  removal efficiency and
associated  cost  are presented  for  actual  operating
technologies employed for utility and  large industrial
boilers. Systems are described in detail, including re-
quirements for retrofitting the technologies to existing
boilers. In general,  performance and costs are more
favorable for new  unit installation  since  space and
operational requirements can be designed into the unit.
Retrofit costs and performance are usually quite site-
specific due both to unique boiler characteristics and
space constraints.

3.2    Coal-Fired  Boilers
Coal-fired  boilers are either pulverized  coal-fired  or
stoker-fired, the latter usually involving small  units.
Most  of the NOX control  technologies  developed  for
coal-fired boilers —  and for  boilers in general — have
been developed for pulverized coal units. Data for these
technologies are  presented below, followed by discus-
sions of technologies developed for stokers.

3.2.1  Pulverized Coal Boilers
The  primary NOX reduction technologies for pulverized
coal boilers have been low NOX burners, various types
of staged combustion, and selective  reduction techni-
ques. Low excess air is easy to implement but may not
bring about the required reductions. These technologies
are presented below.
3.2.1.1   Low Excess Air
The effectiveness of low excess air firing for coal-fired
utility boilers has been summarized for tests on boilers
of the three most prevalent configurations.(14,24) The
data are shown  here in  Table 3-1.

Note from Table 3-1  that for relatively  modest reduc-
tions in  excess air (for example, from 24 percent to 16
percent  excess  air,  or  a reduction of 8  percent for
tangential firing), significant reductions in NOX emis-
sions can be achieved. In most cases higher NOX reduc-
tions are precluded by operational problems that arise at
lower levels of excess air. At very low excess air rates
smoke and excessive carbon monoxide emissions result
from incomplete combustion. Furthermore, depending
on the type of coal fired, slagging and/or corrosion may
increase to unacceptable levels and boiler tubes may
suffer premature failure. Although it is currently a com-
plex matter to predict the minimum  level of excess air
that will permit safe operation, further research in this
area may both define the lower limit and perhaps extend
it further with newer combustion chamber designs.

There is no significant additional cost to implement low
excess air firing in new boilers. (3) In fact, decreasing ex-
cess air can in many cases actually reduce the cost of
operating a  boiler  by  increasing  boiler efficiency as
much as 5 percent. The estimated capital cost to retrofit
a boiler for low excess air firing would be about $400 per
Table 3-1.    Average Reported NOX Reduction with Low Excess Air Firing in Coal-Fired Utility Boilers (14).
                                 Baseline
                                                            Low Excess Air (LEA)
Equipment Type
Tangential"
Opposed wall6
Single wallc

Average (mean)
Number
of
Tests
21
11
23

55
Stoichiometry
to Active
Burners, %
124
126
123

124
NOX Emissions
ppm dry
<5> 3% O2
459
746
624

609
Stoichiometry
to Active
Burners, %
116
118
114

116
NOx Emissions
ppm dry
@ 3% O2
373
660
525

522
Average NOX
Reduction, %
19
12
16
(1)"
16
Maximum NO,
Reduction
Reported, %
42
23
25
(3)"
30
"Burners firing from the furnace corners on a tangent to an imaginary circle in the center of the boiler.
^Burners firing from two opposed walls in the furnace.
cBurners firing from only one wall in the furnace.
^Numbers in parentheses refer to boilers originally designed for coal firing with wet-bottom furnaces.
Note: To convert values in ppm (3% 02) to lb/10' Btu, multiply by 0.0014 for coal and oil, 0.0012 for natural gas. (These factors are approx-
     imate and highly dependent on fuel characteristics.)
                                                    23

-------
MW (1984 dollars), which is mostly for modifications to
the combustion air handling system and windboxes.(25)
A  range of  $640 to $740 per MW (1983  dollars) for
capital cost,  with a negligible annual cost, has also been
reported.(7)  Many operators  require an oxygen trim
system for low excess air firing to closely control the ex-
cess air rate; this will entail additional cost.

3.2.1.2 Burners Out of Service
One method of staging combustion in existing boilers is
to employ burners out of service (BOOS).  Figure 3-1
presents results for  BOOS operation for several  single
wall-fired boilers in terms of NOX reduction versus per-
cent BOOS.  For these tests the total number of burners
ranges from  15 to 24, with those out of service from 2 to
8.  For example,  2 of 16 burners out of service means
12.5  percent  BOOS. The percentage  reductions in
Figure 3-1 represent between  100 and 600 ppm (dry, 3
percent oxygen basis), from baseline NOX emissions of
400 to 700 ppm.
Figure 3-2 shows results for BOOS operation of horizon-
tally opposed wall-fired boilers. Note that with two ex-
ceptions BOOS operation resulted in  NOX emission
reductions of 15 to 30 percent from the baseline level.
The Gaston  Unit 1 boiler was equipped  with specially
designed (low NOX) burners and therefore  did not ex-
perience a dramatic NOX reduction from  BOOS opera-
tion.

Substantial NOX reduction  by BOOS operation has also
been  shown for tangential-fired boilers, as apparent
from Figure 3-3.  Again, there is a reasonably good cor-
relation  between degree  of   BOOS  (percentage  of
Figure 3-1.    IMOX Reduction by BOOS for Single Wall-Fired
            Boilers Burning Coal at 120 Percent Excess Air
            (15,16).
                                                 Figure 3-2.   NOX Reduction by BOOS for Horizontally Op-
                                                            posed Wall-Fired Boilers Burning Coal (15,16).
    60
           Station/Unit
         • Crist 6
         • Edwards 2
         A Mercer 1
    50 I— •Johnston 2 	~~?
         *Widows Creek 5        >£
         ^Shawnee 10         >  *
  - 40
  T3
  0)
  cc
  X
  o
30
     20

              /       /
   -/~~,'—
      */
     10
               15
                  20       25
                    BOOS, %
                                        30
                                           35
                                                     1000
                                                      900
                                                      800
                                                   ON
                                                   *  700
                                                   co
                                                   2


                                                   ^.  600
                                                   Q

                                                   I

                                                   0~  500
                                                   Z
                                                      400
                                                     300
                                                     200
                                                           Open symbols = baseline operation
                                                           Closed symbols = BOOS operation
                                                                                       Four Corners 4
                                                                               Gaston 1
       123        456
                     Boiler Excess 02, %


burners out of service) and NOX reduction achieved.
The units tested range in size from 16 burners (95 MW)
to 56 burners (800 MW).  For this boiler configuration
the most effective BOOS  pattern was observed to be
operation with the top row of burners out of service, a
pattern that simulates overfire air.
Retrofitting a coal-fired boiler for BOOS operation nor-
mally does not involve a  significant capital expense.
However, there are  subtle costs involved  in such a
retrofit that are difficult to predict.  Considerable ex-
perimentation may be required  to find the optimum
number and arrangement of burners to be taken out of
service, although most BOOS patterns consist of taking
burners out of service in the upper regions of the boiler.
In any case, a BOOS design creates fuel-rich and oxy-
gen pockets that essentially stage the combustion. This
not only takes operator and management time but also
requires  testing the  flue gas for NOX  as well as for
smoke and carbon monoxide.  Tests  are necessary to
verify the arrangement  that will minimize NOX while
holding smoke and carbon monoxide emissions to ac-
ceptable levels. Each  case will be different in that there
are no "normal" or "average" combinations of coal pro-
                        24

-------
perties,  boiler layouts,  and  combustion  conditions.
BOOS may also require a boiler derating if the pulverizer
mills cannot supply the additional fuel to the lower (in-
service) burners.  If so, there may be a substantial addi-
tional cost for replacement power.

3.2.1.3  Biased  Firing
Little  performance or cost information is available for
biased firing in coal-fired boilers. The meager data that
are available indicate that NOX reductions on the order
of 7 to 8 percent  were found in limited testing.

3.2.1.4  OverfireAir
Overfire air is a new and retrofit technology for staging
combustion in coal-fired boilers (including  stoker-fired
boilers).  It has been  used extensively, especially for
tangential-fired boilers where  it is offered  for  new
boilers.  A  typical overfire air  retrofit  is shown
schematically  in Figure 3-4.

Limited data are  available on the effectiveness of over-
fire air for single and horizontally opposed wall-fired
boilers. A 22 percent NOX reduction was achieved  in a
test of simulated overfire air  in which the  top row of
burners in a single wall unit was taken out of service.
This mode of operation provided about 16 percent of
the total  air  as  overfire air to  the boiler.  Tests of a
horizontally opposed 350 MW unit showed  NOX reduc-
tions  of 50 percent and higher (from a baseline of 650
ppm)  with  a  significant  (greater  than 50 percent)
amount  of air delivered as overfire air. Although im-
pressive, this testing was limited and further verification
in the field is required.
Figure 3-3.   NOX Reduction by BOOS for Tangential-Fired
            Boilers Burning Coal (15,16).
Figure 3-4.    Typical Retrofit Arrangement for Overfire Air
            (26).
    50
    40
    30
    20
7
    10
/ /
I I
15 20
BOOS, %
Station /Unit
• Barry 2
• Barry 4
ANaughton 3
ANavajo 2
^Widows Creek 7
i l
25 30
                   F - Fuel and air
                   A-Air
                   0 - Overfire air
 Substantial data showing the effectiveness of overfire
 air for NOX control are available  for  tangential-fired
 boilers.  Figure  3-5 shows  the reductions achieved in
 tests at three boilers ranging in capacity from 130 to 800
 MW,  each operating at 120 percent excess air. Note
 that  significant (10 to 30 percent) reductions were
 achieved at relatively  high overfire air rates.  A  1980
 Acurex  Corporation study reported  on  46  tests of
 tangential-fired boilers wherein  NOX emissions were
 measured for the baseline  condition and the condition
 of overfire air. The results are shown in Table 3-2. Note
 from Table 3-2 that diverting about 20 percent of the
 total combustion  air to the overfire air ports resulted in
 an average reduction of 31 percent in NOX emissions.

 Considerable cost data are available for retrofitting over-
 fire air to existing  boilers. Figure 3-6 presents capital
 cost in terms of dollars per kilowatt versus boiler size in
 megawatts. Note that data are from three  different
 sources and that the  actual boiler modifications were
 likely  to be different for each. Therefore a cost range
 has been designated, as the shaded area indicates. Note
 also that the cost data plotted are from three different
 time periods.

 Table 3-3  summarizes capital  and  annualized costs
 (1983 dollars) for retrofitting three model-sized boilers
 with overfire air.  For retrofits, overfire air is in general
 relatively inexpensive;  it mainly involves the installation
 of several  ports above  the  burner  rows  and  the
 associated air piping. Low excess air is the least costly
 option and in larger sizes may actually provide a net
 credit due to increasing the efficiency of the boiler.
                                                                                 25

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Figure 3-5.    NOx Reduction by Overfire Air For Tangential-
            Fired Boilers Burning Coal (7).
                                         Figure 3-6.   Costs of Retrofitting Coal-Fired Boilers for
                                                     Overfire Air (7).
T3
CD
tr
    40
    30
    20
    10
            Station/Unit
          • Comanche 1
          • Barry 2
          A Navajo 2
                      50      75
                     Overfire Air, %
                                      100
                                125
3.2.1.5  Arch Firing
Because this technology involves elemental changes in
the design of a boiler, it cannot be conceived of as a
retrofit technology but rather must be viewed as a
potential "new" technology. Arch firing is a technology
primarily limited to boilers firing difficult-to-burn  an-
thracite coal  and  coke  and a  small  number  of
bituminous coal-fired units of Wisconsin Electric Power
Co.(27) There are few studies comparing the effective-
ness of arch firing and wall firing from which a mean-
ingful  estimate of NOX  reduction could be calculated.
Tests of existing arch-fired boilers (27) have shown that
NOX emissions are on the order of 200 to 350 ppm NOX
(at 3 percent oxygen), which is relatively low for "un-
controlled" NOX emissions. However, the  units tested
were relatively small, ranging in capacity from 80 to 265
MW; most of the units constructed in the future would
be expected to be in a larger size range.
Available data (27) indicate that the total installed cost
for a base  arch-fired boiler (500 MW) is estimated to be
5.4 percent greater than the cost of a comparable wall-
fired unit; an alternate arch-fired boiler was  estimated to
cost 26 percent more than the base wall-fired unit. The
alternate unit selected corresponded to a  larger boiler
due to different geometry, although it too was rated at
500 MW.

3.2.1.6  Low NOX Burners
Burners have been designed, primarily by equipment
and boiler  vendors, that are inherently low in  NOX pro-
                                                        o
                                                           4.0
                                                           3.0
                                            2.0
                                                           1.0
                                                   A Jain, etal. (1972)
                                                   • Bartok, etal. (1969)
                                                   • Shimizu (1975) LADWP
                                                       200     400     600     800
                                                                  Unit Size, MW
                                                                                                    1000
                                          duction,  usually  because of  internal  combustion
                                          staging.  Many of  these burners have been tested  at
                                          laboratory, demonstration,  and  full  scale, with  cor-
                                          responding data for NOX reductions achieved and cost.
                                          The data available  on cost are usually for retrofitting an
                                          existing boiler. The reader is cautioned, however, that
                                          the performance and cost data presented below are for
                                          specific  applications  and are  given as examples  of
                                          achievable results. Particularly for retrofits,  every case
                                          will be  different and more than one NOX reduction
                                          technology   may be  required  in  some  retrofit
                                          applications.

                                          Riley Stoker Corporation has developed and tested the
                                          Controlled Combustion Venturi (CCV) burner for retro-
                                          fitted wall-fired boilers. Figure 3-7 shows results of pilot-
                                          scale tests for the  traditional Riley flare burner and the
                                          CCV burner. The tests were conducted at the EER Cor-
                                          poration test facility at firing rates up to 50 x 106 Btu/h.
                                          The NOX reductions achieved by the CCV burner were
                                          about 55 percent compared to the baseline of the flare
                                          burner.

                                          The effectiveness  of the CCV burner as a retrofit  to
                                          replace  the traditional flare  burner was also tested for
                                          full-scale operating units. A single-wall boiler rated  at
                                          400 MW was  tested before and after replacing the 24
                                          flare burners  with  CCV burners.(5) The  NOX  emission
Table 3-2.    Average Reported NOX Reduction with Overfire Air Firing in Tangential Coal-Fired Utility Boilers (14).

                   Baseline                   Overfire Air (OFA)
Number
of
Tests
Stoichiometry
to Active
Burners, %
NOX Emissions
ppm dry
@ 3% O2
Stoichiometry
to Active
Burners, %
Furnace
Stoichiometry, %
NOX Emissions
ppm dry
@ 3% 02
Average NOX
Reduction, %
Maximum
NOX Reduction
Reported, %
    46
129
454
                                          105
                                          122
                                                                      311
                                                                                     31
                                                                                                  41
                         26

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Table 3-3.   Cost of Retrofitting Coal-Fired Boilers for Overfire Air (7)
            (1983 dollars)
Overfire
Air
New


Retro


MW
250
500
750
250
500
750
Capital
Invest.
$/kW
0.30
0.20
0.15
1.17
0.75
0.60
Annual
Capital
$/kW
0.054
0.036
0.027
0.21
0.14
0.11
Oper.
$/kW
0.005
0.003
0.003
0.02
0.01
0.01
Annual
Fuel Total
$/kW $/kW
0.059
0.039
0.030
0.23
0.15
- 0.12
Electrical
mills /kWh
0.011
0.007
0.005
0.043
0.027
0.022
 rate was reduced approximately 50 percent to levels of
 320 to 440 ppm (3 percent oxygen) while burning a high
 volatile "C" bituminous coal at 22 percent excess air.
 Loss on ignition tests of combustible materials in the
 ash established a decrease in boiler efficiency of only
 0.25 percent.
 Also tested was a 360-MW, horizontally opposed boiler
 with a total of 24 burners.(5) After retrofitting with CCV
 burners the NOX emission level fell from 810 ppm to bet-
 ween 353 and 397 ppm (all on 3 percent oxygen basis).
 Again, no significant adverse effects on boiler perfor-
 mance were noted.
 The Controlled Flow/Split-Flame  (CF/SF) burner has
 been developed by Foster Wheeler Energy Corporation
 and has  been tested on a variety of pilot and full-scale
units. Figure 3-8 presents idealized NOX emissions ver-
sus burner stoichiometry for the CF/SF burner as com-
pared to  the intervane burner which represents the
baseline case for retrofitting  a  Foster Wheeler boiler.
Foster Wheeler has also tested NOX emissions  for a
360-MW front wall-fired boiler and a 525-MW opposed-
fired boiler as well as for a 50 x 106 Btu / h test burner, all
equipped with CF/SF burners.CIO) Although none was
tested before retrofit,  the company claims NOX reduc-
tions of about 60 percent  by retrofitting  with  CF/SF
burners. Currently,  two  domestic utility boilers are
operating  with retrofitted CF/SF burners: a 350-MW
 Figure 3-8.   Theoretical NOX Emissions Versus Burner
            Stoichiometry for the Controlled Flow/Split
            Flame Burner (10).
 Figure 3-7.    Pilot-Scale Test Results for the CCV Burner (5).
  1000
   800
£  600
 ^ 400
O
   200
                                     Riley Flare Burner
                                     with 20% Flue
                                     Gas Recirculation
                 i Distributed Mixing Burner Staged
                             I
                 100       200        300
           Burning Area Heat Release Rate, 103 Btu/h-ft2
                                                 400
                 Controlled Flow Split-Flame Burner
                                                            0.3 -
                                                            0.2
                  90         100         110
                    Burner Stoichiometry, %
                                                                                                           120
                                                                                 27

-------
single-wall-fired unit and a 525-MW opposed-fired unit.
Tests indicate that both units operate at well below the
NSPS limit  of  0.5  lb/106  Btu  for  subbituminous
coal. (10)

Foster Wheeler, in conjunction with EER Corporation
and  EPA, has also developed the Distributed  Mixing
Burner (DMB). Full-scale test results may be available
presently but to  date the bulk of data available are for
research burners  and  in  some   cases  for  research
furnaces.

Babcock  &  Wilcox  Company  developed  the Dual
Register burner early in the history of low NOX burners
and as a result, several thousand of these burners have
been sold domestically,  mostly  for  new wall-fired
boilers. This burner has also been retrofitted and in fact,
the company's NOX emission guarantees are based on
extensive  testing in  a retrofitted boiler.  Considerable
data are available on the emissions and  emission reduc-
tions achievable with this  burner simply because there
are so many currently in use. Figure 3-9 shows the per-
formance  of the dual register burner compared to  the
B&W circular burner  it has replaced. Note that  the
reductions achieved are on the order of 50 to 60 percent
throughout the range of boiler sizes and are nearly all
comfortably below the NSPS level of 0.5 Ib/106 Btu for
subbituminous coal.

Babcock & Wilcox is also, in conjunction  with EPRI,
developing a  retrofit low NOX burner to replace B&W
cell burners. (28) Cell  burners, inherently high  in NOX
emissions, represent a significant segment of the pre-
NSPS pulverized coal-fired boiler population. Each  cell
consists of two  circular burners mounted together to
produce a high-velocity turbulent flame in horizontally
opposed wall-fired boilers.
The company has developed two low NOX replacement
burners, able to be retrofitted into the existing cell. One
is a cell in which the upper burner supplies overfire air
only; the other is a pair of distributed mixing burners. In
pilot-scale testing the former arrangement provided 65
percent NOX reduction (Figure  3-10). In addition to
reducing NOX emissions to below the NSPS level, the
pilot tests of the ash revealed that for both coals tested,
operation with low  NOX  burners  resulted in slightly
lower levels of unburned hydrocarbons, suggesting that
thermal efficiency is preserved after retrofit.(28) This
burner arrangement is currently  being  evaluated in an
actual  operating boiler of 610 MW  capacity,  and  will
undergo further subscale tests in an EPA test facility.

Low NOX burners for tangential-fired boilers have been
developed  primarily by Combustion  Engineering, Inc.,
and their licensee, Mitsubishi Heavy  Industries.  The
Low  NOX  Concentric Firing System  (LNCFS) was
developed by C-E primarily as a  retrofit technology for
existing coal-fired boilers.
In conventional tangential firing, the burners are corner
mounted with their axes tangent to an  imaginary circle
in the center of the boiler.  In LNCFS, the  auxiliary air is
directed at a  larger concentric circle so that the flame
front is stabilized and the devolatilization of the coal oc-
curs in a fuel-rich atmosphere. The retrofitting  involves
modifications to the boiler windboxes alone; therefore,
strictly speaking the LNCFS is  not  really a low NOX
burner. However, modifications  of this type are often
classified as low NOX burners.

Results of full-scale (400 MW) tests of the LNCFS ver-
sus the conventional burner arrangement are shown in
Figure 3-11. Note that NOX reductions on the order of 20
to 30 percent from baseline levels of 460 to 480  ppm are
Figure 3-9.    NOX Emissions for Dual Register Versus Circular Burners in Coal-Fired Boilers (14).
0.8

m 0.6
&
X
o
Z 0.4
0.2
0





i




//
I




































"*.*.



• Circular
Burner

EPA NOX
Emission Limit
1!
Ii
i
!
1
!
I
II
II
V-
1.
Dual Register
Burner
           90   330   470   470   550  550-  550  575   580   600   650   675   700    700   700

                                            Unit Capacity, MW
                        28

-------
Figure 3-10.   Pilot-Scale Results for NOX Reduction by Low
            NOX Cell Retrofit Burners (28).
   2.5
   1.6
df

d
  0.5
                 D Standard cell burner with Ohio No. 6
                 • Standard cell burner with lower Kittaning
                 A Low NOX cell burner with Ohio No. 6
                 A Low NOX cell burner with lower Kittaning
                3.4
                                      4.4
                       Excess 02,
possible.  Even  greater  reductions  can  be achieved
where overfire air is employed in addition to retrofitting
with LNCFS (Figure 3-12). In these tests, potential im-
pacts on boiler efficiency were gauged by unburned car-
bon in flyash. Levels of unburned carbon in flyash were
actually lower after retrofit (on an equivalent NOX emis-
sion basis), indicating no adverse impact of the LNCFS
on efficiency. (6)

MHI  has also  developed the  Low  NOX Pollution
Minimum  (PM)  Burner System to meet stringent NOX
Figure 3-11.   NOX Emissions for the Low NOX Concentric Fir-
            ing System in Coal-Fired Tangential Boilers: No
            Overfire Air (6).
                                      regulations in Japan. The  PM  burner basically divides
                                      the coal/air mixture into fuel-rich and fuel-lean streams
                                      and supplies auxiliary air in an intricately designed wind-
                                      box. The design is a refinement of the SGR burner that
                                      itself was a wall-fired version of the LNCFS concept.

                                      Projections of NOX reductions for a 600-MW boiler and
                                      a 575-MW divided boiler are shown in Table 3-4. Note
                                      the significant NOX reductions  estimated over conven-
                                      tional tangential firing. Case I refers to a retrofit design-
                                      ed  for  minimum  boiler modifications, while  Case  II
                                      refers to a retrofit where maximum NOX reduction was
                                      the goal. The "new unit" was actually Plant A retrofit-
                                      ted in such a manner as to  reflect how the boiler would
                                      be constructed if new.

                                      The cost of retrofitting with the PM burner system is
                                      given later in this chapter.
                                      Figure 3-12.   NOX Emissions for the Low NOX Concentric Fir-
                                                  ing System in Coal-Fired Tangential Boilers:
                                                  Full Overfire Air (6).
                                       m
                                       o
                                       n.
                                       o.
                                                             500
                                           400
                                           300
                                                             200
                                                  Full load (390-420 MW)
                                                  Full overfire air
                                                  • Baseline
                                                  • Postmodification
                                             2.0
                                                       3.0
                            4.0
                        Excess 02, %
                                                                            0.5
                                                                                      6.0
     600


     550

     500
 d

 £  450
 o

 I"  400


     35°
 z
     300
     250
     200
               Full load (390-420 MW)
               No overfire air
               • Baseline
               • Postmodification
        2.0
3.0
                            4.0
                         Excess 02, %
                                       5.0
                              6.0
3.2.1.6.1   Side  Effects of Low NOX Burner and
Staged Combustion
Commercial  methods of reducing  NOX in coal-fired
boilers are often characterized by two conditions poten-
tially  detrimental to  the longevity of  boiler tubes:  a
reducing atmosphere that may promote slagging and
remove the oxidized coating of tubes and expose them
to  accelerated  corrosion;   and  flame  impingement
resulting from longer flames which can overheat tubes
and cause premature failure by thermal stress.

Air staging (BOOS or overfire air)  can potentially result
in increased tube wall corrosion. Proper application and
design can minimize or even eliminate corrosion.(17)

Extensive testing of the corrosion  potential of low NOX
operation has been conducted with major conclusions
as follows:

•  It is  critical that the  burner  and boiler design and
   operating  conditions  avoid sulfidation of tubes by
                                                                                29

-------
Table 3-4.
IMOX Performance for PM Burner System in
Tangential-Fired Boilers (6)
                NOX Guarantee"' ppm
                          % NOX Reduction
Plant A6
Case 1
Case II
New Unit
Plant Bc

190
150
150
160

46"
57"
57d
50*
"Corrected to 3% 02.
*600 MW boiler.
C575 MW divided boiler.
''Based on Plant A emissions of 350 ppm corrected to 3% O2.
"Based on Plant B emissions of 320 ppm corrected to 3% 02.
   flame impingement  of unburned sulfur pyrites and
   corrosion by liquid pyrosulfate.
 •  Proper  selection of materials of construction can
   minimize stress corrosion from alternating oxidizing
   and reducing environments.
 •  Corrosion can  be minimized by selection of certain
   stainless steels and other alloys over carbon steel.

 While corrosion  is the side effect of  most  concern
 resulting from low NOX combustion, there are several
 others, which become constraints on how the unit is
 controlled:

 •  Increased carbon monoxide emissions which may be
   generated by incomplete combustion  at very low ex-
   cess air rates
 •  Smoke  (carbon) emissions which may likewise in-
   crease as a result of  low excess air
 •  Problems associated with flame instability
 •  Limits on flexibility of the combustion unit (changes
   in load)
 •  The presence of carbon in the fly ash.

 These problems may impose limits on fuel switching or
 even require a derating  of the unit.

 3.2.1.6.2   Cost of Low NOX Burners
 Data on the cost of retrofitting coal-fired burners are not
 plentiful and  the  data  that are available are naturally
 highly site-specific.  However,  a  few  examples are
 presented here in order to show the magnitude of the
 cost of such retrofits. In terms of new boilers, the in-
 cremental cost of the low NOX burners themselves is im-
 possible to separate out. Low NOX burners or controls
 such as low excess air, biased  firing, and so on  have
 become state-of-the-art and thus are  offered as stan-
 dard equipment for new boilers at relatively low invest-
 ment cost.
 Figure 3-13 shows the  cost (1983 dollars)  in terms of
 dollars per ton of NOX removed for retrofitting boilers of
 two different  ages with the  Foster Wheeler controlled
 flow/split flame burner. Note that because of increased
 capability to fire  at low loads without significant aux-
 iliary fuel, the costs are presented as a function of "oil
 reduction" in  hours per year, which means the hours
that the original Class 1 ignitors (which fire auxiliary oil
                                                         Figure 3-13.  Offsetting Retrofit Costs of Controlled
                                                                    Flow/Split Flame Burners with Oil Savings*(10).
                                                                               20 Years of
                                                                           Boiler Life Remaining     10Yearsof
                                                                                           ~ Boiler Life Remaining
                                                                                        Breakeven
                                                    0         50        100       150       200
                                                    Reduction in Oil Usage by Auxiliary Oil Burners, h/yr

                                               *This offset is a function of remaining boiler life, reductions in
                                               annual oil usage by auxiliary oil burners (expressed in hours per
                                               year), and the retrofit cost of the controlled flow/split flame
                                               burners (expressed as dollars per ton of NOX removed).

                                             to sustain combustion at low boiler loads) are not fired.
                                             Further note that for the newer boiler, oil reduction in
                                             excess of about 70 hours per year will offset the cost of
                                             retrofitting  and  bring  about a  net  savings at higher
                                             values.

                                             Estimated capital and annual power costs for retrofitting
                                             with PM burners are  shown in Table 3-5 in 1981 dollars.
                                             Note the high capital cost for the extensive modification
                                             (Plant A, Case II) and for the retrofit in a divided boiler
                                             (Plant B). These costs are from a feasibility study (29)
                                             and are only presented as an example. Every retrofit is a
                                             special case with a corresponding cost that may not ap-
                                             ply to any other boiler.
                                             Table 3-5.    Cost of Retrofitting with PM Burners°l20)
                                                         (1981 dollars)
Total Capital
$/kW
Plant A
Case I
Case II
New Unit
Plant B

7.91
15.90
5.44
14.29
Power Costs
mills /kWh

0.22
0.45
0.15
0.40
"Confidence levels ±20%.
                                             3.2.1.7   Reburning
                                             There have been a number of development efforts, in-
                                             itially in Japan, to apply reburning for the control of NOX
                                             from large industrial and utility boilers. The activity in
                                             the United States has extended this technology to other
                                             combustion  sources  and  to  the  consideration  of
                                             simultaneous  S02  control  by  dry  sorbent injection.
                         30

-------
These have been supported by EPA, Department of
Energy  (DOE),  EPRI,  and  GRI.  Several  specific
technologies have arisen such as MACT (for Mitsubishi
Advanced Combustion Technology), an application to
cyclone combustors (Japanese Ministry of International
Trade and Industry)  (30),  an  application to furnaces
(Hitachi Zosen) (31), and the In-Furnace NOX Reduction
(IFNRU32)

The  bench- and  pilot-scale  results have  generally
demonstrated greater than 50 percent reduction of NOX
using between 10 and 20 percent of the fuel for reburn-
ing.(30,32,33,34) A relatively  complete  data base is
available on the impact of the major process variables
from these studies. The data indicate that less reduction
can be achieved at lower initial NOX levels and that the
parameters  within the reburn  zone  control  the
achievable NOX reduction. In particular, the reburn fuel
type can have a significant impact on the level of con-
trol. The nitrogen in the reburn fuel is an impediment to
the  process. Natural gas is an effective reburn fuel
because it has no fuel nitrogen, reacts rapidly so that
short reburn zones are achievable, does not slag or have
burnout problems as with other fuels, can achieve more
reduction in NOX especially at lower  initial values, and
finally, can work at lower temperatures. Pilot-scale tests
with practical times,  temperatures, and  primary fuels
have  generally  demonstrated  over  60 percent
reduction.(35,36) EPA in-house tests have shown that
distillate oil is slightly more effective than natural gas as
a reburn fuel.
Full-scale test  results  are  available  for a  600-MW
tangentially fired boiler (37) firing coal and oil and using
oil as the reburn  fuel. There were five burner elevations
for oil  and two for coal.  Figure 3-14 shows the results
which are for a 90:10 ratio of oil to coal.  Note that NOX
reductions on the order of 40 to 50 percent were found
in these  tests. There are no known  instances of full-
scale testing of  reburning for coal-fired boilers in  the
United States, although a number of studies are cur-
rently underway.

3.2.1.8  Slagging Combustors
Recently  there  has  been  a  significant amount  of
research at  the  laboratory  and  pilot scale concerning
slagging  or  external combustion. The technology has
emerged out  of the field of magnetohydrodynamic
(MHD) power generation where such combustors  are
used to provide heat to ceramic heat exchangers.(38) In
certain applications, especially in  converting gas- or oil-
fired  boilers to  coal  firing, it is advantageous  or
necessary to initiate combustion external to the boiler
and to remove slag from the combustion gas prior to en-
try into the boiler. For boilers designed for oil or gas fir-
ing the use of  coal would result in fouling  of heat
transfer  surfaces and  plugging  of  the  boiler gas
passages, rendering the boiler inoperable in a short time
period. The  benefits which accrue from the retrofit of
coal-fired boilers are  greatly   reduced boiler tube
wastage, NOX and sulfur dioxide emission  reduction.
Figure 3-14.   NOX Reduction by MACT for a 600-MW Coal/
            Oil Boiler (37).
   100
m
o
CD
 O
    80
    60
    40
    20
                     Coal consumption fixed over load range.
                     Oil/Coal = 90/10
          Non-MACT Operation
150 200     300          450

              Boiler Load, MW
                                          600
and greater efficiency that would result from reduced
coal flyash deposits on boiler heat transfer surfaces.
In slagging combustion the initial combustion process is
carried out quickly and under fuel-rich conditions so
that formation of fuel NOX is minimized.
Sulfur oxides can be absorbed in this stage usually by
addition of a calcium-based sorbent. The sorbent reacts
with the S02 to form solids which are removed with slag
or collected in the paniculate emission control device.
Provided a brief cooling period is allowed before the gas
enters the boiler, overfire air can be added to complete
combustion without significant formation of thermal
NOX.

Several  configurations of  slagging combustors have
been  tested at  a pilot scale where the radiant  heat
transfer of a boiler has been simulated. Results of some
tests are shown in  Figures 3-15 and 3-16 on different
configurations.  Note in  Figure  3-15  that the   low
 Figure 3-15.  NOX Emissions from a Slagging Combustion
            Pilot Plant Firing Coal (39).
0 500
S 400
|.300
Q
| 200
a
0 100
0
U.S. NSPS-Bituminous Coal
" U.S. NSPS — Subbituminous Coal
Average Data:
• Burner exit
• Boiler exit (plotted
at burner exit
• stoichiometry)
A • LNSB Goal
200-
3
CL
_C
O)
iooc-
A
i i i i


Q.
-0.4 |
m
-0.2 |
-0.1
      .4    0.5       0.6       0.7      0.8

         Burner Stoichiometric Ratio, Air/Fuel
                                                                              31

-------
Figure 3-16.
   350
INOx Emissions from a Slagging Combustion
Pilot Plant Firing Coal, Oil, and Mixtures (38).
                            • Coal
                            OOil/Coal (1/3 Weight Ratio)
                            DON/Coal (1/1 Weight Ratio)
                            • Oil
                0.8         1.0        1.2
                 First Stage Equivalence Ratio
N0x/S0x Burner (LNSB) program goal of 100 ppm was
not realized in all tests, but results were well below the
NSPS levels. In Figure 3-16, the minimum NOX of about
100 ppm was realized at a stoichiometric ratio of about
0.8 for all fuels (in the primary combustion stage). Fur-
ther pilot-scale research is underway to test the ability
of slagging combustors to simultaneously reduce S02
emissions  by  sorbent injection. This technology is a
long way from commercialization as full-scale tests will
not be completed for several years.  TRW is presently
performing tests on an industrial boiler.

3.2.1.9  Dry  Flue Gas Treatment Technologies
Two  major dry FGT processes —  the  selective  non-
catalytic reduction  process and the  selective catalytic
reduction process — are still in the development stage
in terms of their application to coal-fired boilers in the
United  States. Selective  catalytic reduction has  been
applied extensively in Japan  and is  being planned  for
several European facilities. Figure 3-17 shows results for
a  Japanese utility boiler (175 MW). NOX removal has
been a steady 80 percent and  higher. Note that  max-
imum NOX reductions were found at  an NH3/NOX mole
ratio of  1.0 with little ammonia slip. Also, NOX reduc-
tions averaging about 90 percent were found  in EPA
pilot-scale tests  at a  Georgia  Power  Company
boiler. (40) The pilot  plant  treated a  1,500  scfm
slipstream of flue gas from a 60-MW boiler. It was noted
that when the NH3/NOX ratio was below 1.0, the NOX
reduction achieved  dropped to well below 90 percent.

A number of major  concerns need to be resolved before
this process can be considered totally commercial for
coal-fired boilers in the United  States. These are:

 •   Ammonia slip
 •   Sulfate and bisulfate formation and deposition
 •   Catalyst durability, cost, and reliability
 •   Ammonia and NOX control systems.
Ammonia slip refers to that portion of the ammonia that
passes through the boiler without reacting with nitrogen
oxide. Once excess ammonia has "slipped" through the
NOX control system, it can react with sulfur trioxide to
form ammonium bisulfate. This  compound is a par-
ticulate that can foul the combustion air preheater and
could conceivably, in extreme cases,  jeopardize par-
ticulate compliance. Therefore, ammonia slip must be
controlled;  accordingly, Japanese  utilities employing
SCR on their boilers usually specify strict limits for their
vendors on the amount of ammonia permitted to slip.
Some Japanese boilers continuously monitor for am-
monia in  the flue gas.(14)

There are cost data and calculations available for SCR
as applied to coal-fired boilers. One example, shown in

Figure 3-17.   Test Results for SCR on a Coal-Fired Boiler (2).
                                             >; 100

                                             .1
                                             o
                                             c  80
                                             .2
                                             I  60
                                                350
                                                300
                                                250
                                             ^ 200
                                              §
                                              I  150
                                             O
                                              n
                                             z
                                             O 100
                                                 50
                                                             Unit load = full load
                                                             Flue gas temperature = 340C
                                                             3% 02 concentrations assumed
                                                      -Inlet
                                                      Outlet NOX
                                                      Outlet NH,,
                                                  0.7        0.8        0.9       1.0
                                                                NH3/NOxMole Ratio
                                                                                            1.1
                         32

-------
 Figure 3-18, is the projected cost of an SCR retrofit for a
 300-MW  tangential-fired boiler relative to other NOX
 control technologies. Note the distinct cost disadvan-
 tage, but nevertheless, the NOX removal efficiency ad-
 vantage  represented  by  SCR   compares to  other
 technologies employed more frequently for tangential-
 fired boilers.
 Selective noncatalytic reduction,  as represented by the
 Exxon Thermal DeNOx  process, reportedly costs less
 than SCR but NOX removal is significantly lower. Table
 3-6 presents vendor-supplied data on capital cost and
 cost-effectiveness for the Thermal DeNOx process. The
 costs, which are in 1983 dollars, were developed by the
 vendor for a hypothetical, 500-MW boiler.  The design
 NH3/NOX mole ratio was 1.5.

 Table 3-6.    Capital Cost and Cost-Effectiveness of Thermal
            DeNox Process (48) (1983 dollars)
                                        Table 3-7.    Economic  Evaluation  of  SCR  for  Coal-Fired
                                                    Utility Power Plants: 80% NOX Removal (42)
NOx"
300 ppm
600 ppm
Investment
$/kW
19
25
Cost Effectiveness
mills /kWh $/lb NOX Removed
2.03 0.57
2.94 0.41
"Initial (before SCR) NOX concentration at 3% 02.

An EPA-sponsored economic evaluation  for coal-fired
utility power plants included SCR for NOX control.(42)
The SCR systems consist  of two trains of insulated
reactors. An  ammonia storage and handling system in-
jects  an ammonia/air mixture  in the inlet duct. The
catalyst life is assumed to  be  1 year. Table 3-7 sum-
marizes the capital investment and annual revenue re-
quirements.

The most important capital and annual cost is for the
catalyst. Other than the catalyst, the main factor affec-
ting NOX control costs is the flue gas volume which
determines the fan and ductwork costs and the catalyst
volume.
Coal MW
East 200
East 500
West 200
West 500
West 200
West 500
S02 Control
Limestone FGD
Limestone FGD
Lime Spray Dryer
Lime Spray Dryer
Limestone FGD
Limestone FGD
Capital
Investment
$/kW"
103.1
83.7
121.0
100.2
121.6
96.1
Annual
Revenue*
mills /kWh
8.8
8.0
10.6
9.6
10.1
9.0
"1982 dollars.
b1984 dollars.
                                        3.2.1.10  Wet Flue Gas Treatment
                                        Many processes have been proposed for simultaneous
                                        removal of SO* and NOX. However, there are no data on
                                        their  effectiveness for  full-scale  coal firing.  Limited
                                        testing by the Pittsburgh Energy Technology Center has
                                        shown  that  NOX  removals  of  60 to 70 percent are
                                        achievable along with 90 percent removal of SOX.(43)

                                        No cost data on wet flue gas treatment  processes for
                                        actual coal-firing installations are available. Model plant
                                        cost estimates are available for several processes.


                                        3.2.2  Stoker-Fired Boilers
                                        The primary  NOX reduction technologies that have been
                                        applied to stoker-fired boilers are overfire air control and
                                        flue gas recirculation. The former has traditionally been
                                        employed to reduce smoke emissions from stoker-fired
                                        boilers while the latter has recently been proposed for
                                        the same purpose  but has the added benefit of reducing
                                        NOX emissions. Exhaust gas recirculation reduces fuel
                                        NOX  by lowering oxygen concentrations  in the  bed
                                        where fuel nitrogen is evolved.
Figure 3-18.   Incremental Capital Cost of SCR and Other NOX Control Technologies for a New Tangential-Fired Boiler (26).
 x
 o
 Q.
 Q.
    20
    15
    10
                                                 (80-90)
                                         (40-60)
                                (45-55)
                (15-20)
                        (20-30)
          T-
         Firing
         Base
T-Firing
w/OFA
LNCFS
w/OFA
  PM
w/OFA
MACT
w/PM
&OFA
                                 SCR
                                        Baseline
                                                  NOX removal in parentheses.

                                                  T-Firing Tangential firing
                                                  OFA   Overfire air
                                                  LNCFS Low NOX concentric firing system
                                                  *PM   Pollution minimum burner
                                                  *MACT Mitsubishi advanced combustion technology
                                                  *SCR   Selective catalytic reduction system
                                                                  *C-E/MHI licensed technology
Based on material and construction costs for a new
300 MW coal-fired unit.
SCR system costs are based on 80% NOX removal.
SCR system costs do not include NH3 tank farm
equipment or external structural support steel.
These cost approximations may change depending
on specific unit design requirements.
                                                                                33

-------
 3.2.2.1  Overfire Air
 NOx  reductions of between 10 and 25 percent have
 been reported for employing additional overfire air ports
 (44);  existing overfire air ports are designed primarily for
 smoke control and may  not be optimally located for
 control of  NOX  emissions.  This  method is severely
 limited in that redirecting a large portion of air from the
 bed to the overfire ports reduces the cooling effect of
 the air on the grate and disturbs the natural staged com-
 bustion of the stoker.

 3.2.2.2  Flue Gas Recirculation
 Flue  gas recirculation, also called  stoker gas recircuta-
 tion in this instance, has been suggested for application
 to stoker-fired boilers. Full-scale testing of stoker-fired
 boilers is reported (45)  in which slight NOX reductions
 were achieved for flue gas recirculation  in spreader
 stokers. The boiler, rated at 100,000 Ib/h of steam, fired
 Western Kentucky coal at excess oxygen levels of 8 to
 10 percent.  It was found that in addition to paniculate
 emission reduction (about 40 percent) and efficiency in-
 creases (6 to 7 percent), a side benefit was  reduction in
 NOX  emissions.  Since the recirculated gas is injected
 along with the primary combustion  air, the technique
 results in lower excess  air which in  turn reduces both
 fuel   NOX and thermal  NOX. Figure 3-19  shows  test
 results indicating that NOX emission levels approaching
 100 ppm (3 percent oxygen basis) are achievable. Note
 that NOX emissions for a stoker-fired boiler are relatively
 low to begin with; note further that  the modified (flue
 gas recirculation) system results in lower excess oxygen
 rates  and hence reduced NOX emissions.

 No cost data for either overfire air or flue gas  recircula-
 tion for stoker-fired boilers are available.

3.3   Oil- and Gas-Fired Boilers
 Many of the techniques discussed above for reducing
 NOX emissions from coal-fired boilers  are also applicable
                                                    to oil-fired and gas-fired utility and industrial boilers of
                                                    comparable size. Most of the techniques that have been
                                                    used are those that reduce peak flame temperatures. A
                                                    discussion of available data on the effectiveness and
                                                    cost of these techniques follows.

                                                    3.3.1   Low Excess Air
                                                    Modest (average 11  percent)  NOX reductions can be
                                                    achieved by lowering excess oxygen to the vicinity of
                                                    2.5  percent  for  combustion of residual  and distillate
                                                    oils.(44) A side benefit is an increase in boiler efficiency;
                                                    however, a possible detriment  is increased emission of
                                                    carbon monoxide, hydrocarbons, particulates, and visi-
                                                    ble plume.

                                                    The  reductions  achievable  for gas-fired,  water-tube
                                                    boilers  are  also  modest, in  the  range  of  3  to  15
                                                    percent. (44)  However,  the technology  is  desirable
                                                    because it is easy to implement, can be combined with
                                                    another technology, and again  has the added benefit of
                                                    increasing boiler efficiency. The excess oxygen can be
                                                    safely  reduced  to about 2 percent  in  most boilers
                                                    without jeopardizing  carbon  monoxide and paniculate
                                                    compliance.  Figure 3-20 shows the results of tests of a
                                                    110-MW gas-fired  utility boiler, where NOX emissions
                                                    were reduced by over 30 percent by lowering oxygen in

                                                    Figure 3-20.  IMOX Reduction by  Lowering Excess Air in a
                                                               Gas-Fired Utility Boiler (46).

                                                          11,000
                                                          10,500
                                                          10,000
Figure 3-19.   NOX Reduction Due to Flue Gas Recirculation
            in a Stoker-Fired Boiler (45).
    500
 Q


 Q.
 Q.
400 -
    300
 O  200 -
    100
                         6         8
                       Excess Oj, % Dry
                                                             Q

                                                             Q.
                                                             Q.
                                                         8
                                                         v>
                                                         c
                                                          x
                                                         O
                                                            260
                                                                240
                                                                220
                                                                200
180
                                                                 160
                                                                140
                                                                      0.5    1.0     1.5
                                                                           02 in Flue Gas, 9
                                                                                           2.0
                                     2.5
                         34

-------
 the flue gas from 2.2 to 0.6 percent (corresponding to
 about 2.8 percent excess air).(46) At oxygen  levels in
 flue gas of about 0.6 percent and lower, flame instability
 and combustibles in the flue gas were found, making
 this a practical lower limit for reducing excess air on that
 boiler.(46) Any  reduction in excess oxygen should be
 made  only after evaluating a specific application and
 determining that a potential safety hazard will not arise
 at the lower oxygen  level.

 3.3.2  Burners Out of Service
 This technology is only available as a retrofit  and ob-
 viously only applies to  boilers with more than  one
 burner. Some  utility  and  industrial boilers  burning
 residual  fuel  oil or  natural  gas  have  used this
 technology. NOX reductions range from  10 to over 40
 percent (44) and of course are highly  dependent on
 whether or not the BOOS pattern tested is the optimum
 pattern.  Figure  3-21 shows results of  testing  for  a
 110-MW  gas-fired utility boiler in which BOOS was
 tested in  combination with opening of an  overfire air
 port to further enhance the BOOS effect. A potential
 drawback to this technology is possible derating of the
 boiler unless modifications to the fuel piping are made
 so that the design heat input can be maintained after
 retrofit. Heat rate may also be increased with BOOS.

 3.3.3  Reduced Combustion Air Preheat
 This technique requires extensive modifications to the
 air and flue gas handling systems of a boiler and  is ob-
 viously applicable as a retrofit only for boilers employing
Figure 3-21.  NOX Reduction by BOOS for a Gas-Fired Utility
           Boiler (46).
  100
   90
fc-
Q  80
£  70
   50
       Air only to one bottom burner
           1.2% 02 in flue gas
               100 MW
              Air only to one top burner
                 1.1 % O2 in flue gas
                     95 MW
               20         40
                   NOX Port Opening, %
                                     60
80
 combustion air preheaters. The best application for this
 technology would probably be a new boiler where it is
 necessary  to  include heat  recovery equipment to
 preserve the thermal  efficiency of the  boiler.  The
 technology has been tested on a limited basis for oil-
 fired and gas-fired boilers.(44)  The  NOX reductions
 demonstrated for firing residual oil ranged from 5 to 16
 percent; results of only two tests for gas-fired boilers in-
 dicate NOX reductions of perhaps 30 percent are possi-
 ble  with a combustion air temperature decrease of
 about 50C OOF). Unless alternate heat recovery equip-
 ment is used to  minimize  stack losses, this  technique
 usually produces unacceptable efficiency penalties.

 3.3.4   Flue Gas Recirculation
 As with reduced  combustion air preheat, flue gas recir-
 culation is difficult to retrofit  because of  extensive
 modifications to air and flue gas handling systems. The
 amount of flue gas that is typically recycled is in the
 range of 15 to 20 percent, although levels as high as 45
 percent have been  used for gas firing.(44) The propor-
 tion is limited in oil-fired boilers by the onset of flame in-
 stability; this is less of a problem with gas-fired boilers if
 other than ring burners are employed.

 Testing  of this technology for  oil-fired  and  gas-fired
 boilers has not been extensive. However, preliminary in-
 dications are that substantial NOX reductions can be
 achieved. For example, tests for residual oil firing show-
 ed NOX reductions of 15 to 30 percent while results for
 firing distillate oil  (one boiler only) ranged from 58 to 73
 percent. Tests of three gas-fired boilers showed  NOX
 reduction ranging from 48 to 86 percent.

 3.3.5  Low NOX Burners
 Several burner manufacturers have for some time been
 engaged in developing and  providing low NOX burners
 for oil- and gas-fired  boilers. In some instances the
 burners thus developed are modifications of pulverized
 coal burners in which the basic principles of air or fuel
 staging have been employed. Many of these low  NOX
 burner designs have been licensed  for sale  in Japan
 where operators  of oil- and  gas-fired  utility and in-
 dustrial boilers in general face more stringent NOX emis-
 sion regulations than their U.S. counterparts.

 Babcock & Wilcox has developed the Primary Gas-Dual
 Register Burner (PG-DRB)  for oil-fired and  gas-fired
 boilers. In this burner—which is a modification of the
 coal-firing DRB—the primary air zone is surrounded by
 a primary gas recirculation zone.  Here, recirculated flue
 gas shields the flame and reduces oxygen  availability.
 The company claims NOX emission reductions of 65 per-
 cent for oil and 75 percent for gas firing, as compared to
 conventional circular burners.(41) The field experience
 with this type of  burner includes utility as well as in-
 dustrial  boilers, primarily in Japan. There are 114  PG-
 DRB's firing oil in  four generating stations  in Japan
 ranging in size from 175 to 600 MW; 176 PG-DRB's fire
gas in six stations ranging in size from 175 to 1,000 MW.
The  total  capacity covered  by these burners is  4,700
 MW.
                                                                              35

-------
Coen Company, Inc. supplies low NOX burners for oil or
gas firing in  industrial boilers.(47) Two basic types of
staged air burners are offered: the front wall arrange-
ment that is  especially suited for residual oil (high fuel
nitrogen); and the  side wall arrangement  that is well
suited for gas firing.  The company claims NOX reduc-
tions of 25 to 30 percent for oil firing  and 35 to 40 per-
cent for gas firing, employing these burners. The com-
pany literature reveals a total of 11 installations ranging
in size from one burner and 20,000 Ib / h of steam to four
burners and 400,000 Ib / h of steam that employ this type
of burner. The guaranteed or actual NOX emissions for
these units are 0.1 lb/106 Btu and less for  natural gas,
and 0.2 to 0.3 lb/106  Btu for oil.(47)

3.3.6 Dry Flue Gas Treatment
Figure 3-22 shows results of tests of the Exxon Thermal
DeNOx process at full load on a 235-MW oil-fired utility
boiler in California. The figure shows that NOX removals
of over 50 percent were achieved at the full load condi-
tion. At partial load,  the  change in convective section
temperature  reduced the  NOX reduction efficiency to
below 50 percent. There was also significant ammonia
slip during these tests. Exxon reports that the ammonia
compounds  formed from slippage do not  cause unac-
ceptable corrosion or preheater fouling. Deposits form-
ed can  be  removed from the  system  by periodic
washing with water.(48) Exxon is continuing to develop
the process to improve efficiency.
Catalytic technologies have been tested and used ex-
tensively in Japan for coal-, oil-, and gas-fired industrial
               Figure 3-22.  NOX Reduction by SNR for Oil-Fired Utility
                           Boiler (48).
                   80
                c
                o
                1
                •o
                I
                o
                   60
40
                   20
                     1.0     1.2      1.4       1.6       1.8
                                NH3/Initial NOX Concentration
                                             2.0
                boilers.  Processes with fixed  beds and moving  beds
                have  been  tested.  Performance  data  for actual
                operating systems are available; some representative
                results for oil-fired boilers are shown in Table 3-8.  Per-
                formance data for gas-fired boilers are also available in
                which NOX removal efficiencies of 90 percent have been
                realized  over operating periods  of several thousand
                hours.(43)

                An SCR system was tested that handles half of the flue
                gas from a 215-MW gas-fired utility boiler of Southern
                California Edison Company.(49)  The system  attained
                the design goal of 90 percent NOX  reduction in 18,000
                hours of operation;  however, it is not clear  that  the
 Table 3-8.    IMOX Removal in Oil-Fired Industrial Boilers with Selective Catalytic Reduction (43)
  Operation Parameters of Major Plants
Operation Data of a Commercial SCR
       Plant for Dirty Gas
                         SCR Plant by Mitsui
                    Engineering and jhipbuilding Co.
Completed
Plant site
Gas source
Capacity (NnWhr)
Load factor (%)
Pretreatment of gas

Reactor inlet
NOX (ppm)
SOX (ppm)
Dust (mg/Nm3)
02 (%)
Reactor type
Reaction temp.
NOx/NHj ratio
Catalyst No.
SV (hr1)
NOX removal (%)
Pressure drop by SCR
reactor (mm H20)
Catalyst life
11/75
Yokkaichi
Oil-fired boiler
440,000
50-100
EP", FGD,
heating

150
80-130
30-100
3.2
Fixed bed
420
1.0
304
10,000
80*

160
1 year
Gas for SCR (NmVhr)
Fuel
Load fluctuation (%)
Stack height (ml
Inlet gas composition
02 (%)
SOX (ppm)
NOX (ppm)
Particulates after EP
(mg/Nm3)
FGD unit
SV (rr'1
Temperature (C)
NOX removal (%)
NH3/NOxmol ratio
Leak ammonia (ppm)
Type of reactor
Plant completed



300,000
Oil IS = 0.7%)
60-100
140

6
400
200

10-20
Scheduled
5,000
320
Over 90
1.0
10-20
Moving bed
10/76



Capacity (NnWhr)
Gas composition
NOX (ppm)
SOX (ppm)
Dust (mg/Nm3)
Catalyst and reactor
Catalyst carrier
Catalyst shape
SV (hr1)
Temperature (C)
NrVNOxmol ratio
NOX removal (%)
Total pressure drop
(mm H20)
Leak NH3 (ppm)
Operation start
Plant cost (106 yen)




220,000

150
300
100-150

TiO
PP
4,000
350-400
1.0
Above 90

180
Below 10
7/77
260




  "Electrostatic precipitator.
  6lncluding leakage in heat exchanger.
  Note: At 8/9/85 exchange rate of 237.70 yen per U.S. dollar.
                          36

-------
system can achieve the design of 10 ppm maximum am-
monia slip.  During the test period the boiler was fired
with  oil  for periods of time.  During these  periods,
however, "heavy" deposits of ammonium bisulfate and
iron sulfate were found in the air preheater. At its worst,
this condition resulted in an increase in pressure drop
through the air preheater of 50 percent.(49)

The estimated cost for a Thermal DeNOx process for a
200,000  Ib/h  oil-  or gas-fired  industrial  boiler  is
available.(49) Table 3-9 shows  the  estimated annual
operating costs for this application. The total invest-
ment cost is estimated to be $389,000. If the system is
assumed to have  a  useful life  of 20  years, the annual

Table 3-9.    Annual Operating Cost Estimates  for Thermal
            DeNOx on a 200,000  Ib/h  Oil-Fired  Industrial
            Boiler (30) (1982 dollars)
                    Annual            Unit      Annual
   Cost Item       Consumption"        Cost, $     Cost, $
Ammonia6
Electric powerc
Steamd
Maintenance
(Material and Labor)"
Total
164 t
55 MWh
3,890 t



220/t
50/MWh
13.50/t



36,080
2,750
52,515

7,560
98,905
"Assumes 65% load factor.
^Includes ammonia for direct injection.
""Includes power requirement for ammonia vaporizer.
dLow pressure steam (0.1 MP ag minimum) for carrier.
"Assumed to be 7% of direct investment cost.
capital-related cost would be $45,690 at a 10 percent in-
terest  rate, and thus the total  annualized cost of  the
DeNOx system would be about $160,000, including a
small percentage  of capital cost for insurance, taxes,
and administration.

Table  3-10 shows Japanese  data  (43) on capital and
operating cost of  selective catalytic reduction systems
for oil-fired and gas-fired boilers. The smaller flowrate
would correspond to an industrial boiler while the large
flowrate is  more  typical of a  utility boiler. Note  the
economy of scale evident  in the  capital cost figures
while the operating cost is much closer  to  linear with
flowrate.

Cost data are also available (49) for an SCR system  ap-
plied to gas firing. The data are in the  form of 20-year
levelized costs and are for combustion of oil.  The cost is
a strong function  of the unit's capacity factor  ranging
from greater than $0.0607 kWh at a  capacity factor of 30
percent, down to $0.010/kWh at a capacity factor of 80
percent. (49)
                                                         Table 3-10.
  Gas Flow
 Rate, Nm'/h
             Capital and Operating Cost Data for Selective
             Catalytic Reduction Systems for Oil-Fired and
             Gas-Fired Boilers (43) (1981 dollars)
Capital Cost, $
Operating
 Cost, $
     50,000
   1,200,000
  0.5 x 106
  5.0 x 106
0.2 x 106
3.5 x 106
                                                                                37

-------

-------
                                              Chapter 4
                                   Performance and Cost Data:
                               Packaged Boilers Firing Oil or Gas
 4.1   Introduction
 This chapter presents available data on the NOX removal
 efficiency  and associated cost of those technologies
 employed for smaller, packaged boilers that fire oil, gas,
 or both. Much of the  material in the  latter parts of
 Chapter 3 pertaining to large industrial oil-fired and gas-
 fired boilers also applies to packaged boilers. However,
 many of those technologies have limited application to
 smaller boilers. These limitations will be discussed in
 this chapter.

 Packaged boilers are for the most part industrial rather
 than utility and are small. There has not been a great
 deal of research and  development  of NOX control
 technologies for these boilers. NSPS were proposed in
 June 1984, but have not yet been promulgated.  State
 and local regulations that may apply usually only limit
 emissions of particulates and sulfur dioxide.

 Where  low NOX  technology has been required  for
 packaged boilers, the normal procedure has been to go
 directly to a low NOX burner. On a new or retrofit basis,
 low NOX burners are usually straightforward to imple-
 ment (packaged   boilers  normally  employ  only one
 burner) and relatively cost-effective compared to more
 complicated technologies of lesser NOX  reduction effi-
 ciency.  A few other  technologies have received limited
 attention, however, and these are discussed first.

 4.2  Reduced Combustion Air  Preheat
 This technology  is  available for use with  packaged
 boilers  of  the  water-tube design but,  as  with  large
 boilers,  requires a combustion air preheater. Fewer than
 20 percent  of  packaged boilers have preheaters;  most
 use economizers for heat recovery. Limited data show
 NOX reductions in the range of 5 to 16 percent, which is
 the same for industrial boilers in general.(44) To recover
 lost  thermal  efficiency  boilers equipped  with  this
 technology  (new  or retrofit) require  heat recovery
 systems. Due  to this  severe energy  penalty,  this
 technology is not expected to proliferate, especially in
 view of  the ease of implementing low NOX burners and
the much greater  NOX reduction achievable.

 4.3   Flue Gas  Recirculation
 Flue gas recirculation is a technology available for both
fire-tube and  water-tube  packaged boilers.  It  is  a
technology that is being increasingly implemented on
 packaged units. Tests have reflected a NOX reduction
 ranging  from 15 to 30 percent for residual oil, 58 to 73
 percent for distillate oil, and 48 to 86 percent for gas-
 fired  boilers. (44)  For gas-fired  units the technique is
 more effective with water-tube boilers than fire-tube
 boilers.

 4.4   Low NOX Burners
 In Chapter 3 a discussion of low NOX burners for oil and
 gas firing was presented as part of the material on utility
 and large industrial boilers. In large part, that discussion
 also applies here for packaged boilers.

 Several burner manufacturers have designed low NOX
 burners  for oil and gas firing  that may be used  in
 packaged boilers.  Particularly applicable are the data
 from  Coen Company, Inc.(47) in which two basic types
 of  staged  air low  NOX  burners  are discussed. To
 reiterate, these burners are  claimed to  be capable of
 NOX reductions of 25 to 30 percent (oil) and 35 to 40 per-
 cent (gas). Of the eleven installations mentioned, seven
 are relatively small, one-burner, packaged units. This in-
 formation is summarized in Table 4-1.

 As pointed out earlier there are  a  number of burner
 manufacturers offering low NOX burners for small oil-
 and gas-fired  boilers. Although performance data are
 scarce, many manufacturers are  agreeing to guaranteed
 emission levels comparable to the rather stringent  levels
 of the proposed industrial NSPS.
Table 4-1.    IMOX Emission Performance for Low NOX Burners
            in Single-Burner Oil- and Gas-Fired Boilers (47)
 Boiler Capacity, Ib/h
Fuel
Guaranteed or Actual
   NOX Emission
20,000
68,200
80,000
55,000
30,000
100,000
50,800
Refinery or
natural gas
Natural gas or
No. 2 fuel oil
Refinery or
natural gas
Natural gas or
No. 2 fuel oil
Natural gas or
No. 2 fuel oil
Natural gas or
No. 2 fuel oil
Natural gas
70 ppm (@3% 02)
75 ppm (@3% 02)
0.15lb/10' Btu
0.09lb/106Btu
0.12lb/10" Btu
0.12 lb/106 Btu
0.08 Ib/ 10' Btu
Note: To convert emissions in lb/10' Btu to ppm for firing natural gas,
    multiply by 833.
                                                  39

-------
EPA has developed a low NOX heavy oil  burner  that
generates no more than 75 ppm NOX regardless of the
fuel nitrogen content. This precombustion  type burner
has been applied  only  to an enhanced oil recovery
steam generator rated at 60 x 106 Btu/hr. The precom-
bustor is operated fuel rich at very high temperatures to
take advantage of very low NOX equilibrium  levels.
Burnout air is added at the precombustor outlet to com-
plete the combustion process at lower temperatures.
In addition, Alzeta Corporation, under contract to EPA,
has developed  a "fiber" low NOX burner for gas-fired
fire-tube boilers. Flame temperatures  are kept  low
because a substantial portion of the heat is  provided by
radiant transfer.

The fiber burner has been demonstrated on gas-fired
fire-tube boilers ranging in rating from 245 to 980  kW.
Results  are shown in Table 4-2.  Note that substantial
reductions in NOX emissions (on the order of 80 percent)
are possible  at varying  boiler loads.  Earlier tests  (51)
disclosed that 10 percent excess air was the optimum
operating point. Below this level, carbon monoxide
emissions were excessive and above this level, efficien-
cy was compromised. The carbon monoxide emissions
at 10 percent excess air were comparable to those for a
conventional burner.

4.5   Other Technologies
Several  other technologies are available for packaged
boilers but have not been demonstrated. Reasons  may
include doubts about cost-effectiveness, lack of interest
due to the availability of alternatives, or technical limita-
tions.  Low  excess air  is  available and  readily  im-
plemented. As with overfire air for stoker-fired boilers,
however, low excess air for packaged boilers has tradi-
tionally  been employed for a  reason other than NOX
control (in this case for fuel savings) with reduction of
NOX emissions as a side benefit.

Typically,  an oxygen  trim  system  has  been used to
balance oxygen  against carbon monoxide and smoke
emissions. Either oxygen or  carbon monoxide in the flue
gas is monitored to approach  the lowest practical ex-
cess air level while still complying with any applicable
regulations on particulates (smoke) and carbon monox-
ide. At this low excess air level  (generally about 2.5 per-
cent), NOX  emissions  are  reduced approximately  11
percent. (44)

Tests performed  on a package boiler simulator  and a
commercial  fire-tube boiler, both  rated at 0.73 MW or
2.5 x 106 Btu/hr, have shown that reburning can effec-
tively reduce NOX by 50 percent or greater with minimal
facility  modifications.(19)  However,   for very  low
primary flame NOX levels (less than 200 ppm), reburning
fuel nitrogen content is a limiting factor. Reburning with
a  low nitrogen  content fuel  such  as  natural  gas or
distillate oil  may be necessary. Selective noncatalytic
reduction is  offered commercially  and has been applied
to several packaged boilers and enhanced oil recovery
steam generators in California.
 Table 4-2.    NO, Emission Reduction for Gas-Fired Fire-Tube Boiler with a "Fiber" Low NOx Burner" (50)
Site
Alzeta Lab
Santa Clara, CA
York-Shipley
Boiler Test Bay
York, PA
Vandenberg AFB
CA
Peter Paul Cadbury
York, PA
Hall Chemical Co.
Wickliffe, OH
Boiler
Size
kW
245

588


392

588

980

Burner Type
Conventional
Fiber
Conventional
Fiber

Conventional
Fiber
Conventional
Fiber
Conventional
Fiber
Excess
Air
%
16
10
15
10

55
10
20
7
7
13
CO
ppm
11
10
10
10
240
0
400
35
1,000
35
NO
ppm
57
10
NT
NT
NT
NT
NT
20
80
18
 "All results at high fire conditions, emissions corrected to 0% 02-
 60n segmented burner.
 'Three different burners employed.
 Note: NT =  not tested
      NA = not applicable.
HC
ppm
0
10
NT
NT
NT
NT
NT
NT

NT
NT


Boiler
Eff.
%
82.8
82.3
85.0
85.8
81.0
82.3
83.2
84.0

82.7
83.7


Hours of
Operation
NA
500*
NA
2,000
NA
3,800
NA
3,450
2,500
NA
3,450'
2,500C
1,500C
                         40

-------
                                               Chapter 5
                                   Performance and Cost Data:
                     Gas Turbines and Stationary Reciprocating Engines
 5.1   Introduction
 Available data on the effectiveness and cost of NOX
 reduction technologies for  turbines and  engines are
 presented in this chapter. With the exception of selec-
 tive catalytic reduction technologies,  the  techniques
 presented are unique to these sources and have not
 been discussed in Chapters 3 and 4.

 5.2   Gas Turbines
 The two primary methods of NOX reduction that  have
 been employed for gas turbines are water/steam injec-
 tion  and selective  catalytic  reduction. The  former
 technology is the more advanced in the United States;
 the latter has been used extensively in Japan for several
 types of sources, including gas turbines, and it has been
 used or tested at a few U.S. installations.

 5.2.7  Water/Steam Injection
 Nearly  50  percent  of the gas  turbines in California
 employ water/steam injection for NO* reduction.(52) A
 water injection system consists of nozzles mounted in-
 side the combustor, a proportional controller to ensure
 the correct injection rate, a  pump, and the associated
 piping. Typical water- or steam-to-fuel ratios are 0.21:1
 to 1:1  for water and 1:1 to 2:1 for steam. Water for in-
 jection  must meet  the purity  requirements of boiler
 feedwater in order to avoid corrosion in the turbine. (24)
 The reference also reports that for water-to-fuel ratios in
 the range of 1:1, NOX reductions up to 75 percent are
 realized. This is  basically confirmed by data shown in
 Figures 5-1 and 5-2. (53) Increased (less than 5 percent)
 fuel consumption is a drawback.

 Water/steam injection is only effective in reducing ther-
 mal IMOX. Therefore, it is not  recommended for turbines
 combusting fuels with significant fuel-bound nitrogen
 such as coal-derived liquid, shale oil, and high-nitrogen
 residual oil.

 A by-product of water/steam injection is a modest (1 to
 11  percent)  increase in  power output but  a slight
 decrease in  turbine efficiency.(53)  It is  difficult to
generalize on turbine wear and maintenance problems
because the studies (53) do not indicate any discernible
trend. Suffice it to say that increased turbine wear and
more frequently  required  maintenance  may be conse-
quences of water/steam injection in rare instances. The
formation of ice fog could be a deterrent to the use of
this  technology in populated areas  located in cold
climates, such as Alaska.(53)

Figure 5-1.   NOX Reduction by Water or Steam Injection:
           Gas Turbine Firing Natural Gas (53).
3  50 -
cc
O
            0.4
 0.6     0.8    1.0
Water-to-Fuel Ratio, Ib/lb
1.2
1.4
Figure 5-2.   NO* Reduction by Water or Steam Injection:
           Gas Turbine Firing Distillate Oil (53).
    0.2     0.4     0.6     0.8     1.0
                 Water-to-Fuel Ratio, Ib/lb
                      1.2
                             1.4
                                                   41

-------
Another possible disadvantage is an increase in emis-
sion of carbon monoxide. For turbines operating at base
load with water-to-fuel ratios of 1:1, CO emissions are
approximately 300 ppm, which is about five times the
baseline level.(52) However, for these units operating in
California,  the  carbon monoxide emissions are well
below  the  limit  of 2,000  ppm.  (These concentration
levels assume a 3 percent oxygen  basis.) In any case it is
difficult to generalize on this point because tests are not
consistent with turbine size and fuel type.(53)

5.2.2  Selective Catalytic Reduction
Extensive  testing of  selective catalytic  reduction  has
been carried out in Japan for actual operating gas tur-
bines. Figure 5-3 presents data for the Kawasaki Power
Station Number 1 combined cycle turbine which is rated
at a total of 141 MW (97 MW prime turbine plus 44 MW
steam  turbine).  Note  that at all  turbine loads  greater
than 25 percent the NOX reduction efficiency is well over
80  percent  and  ammonia emissions—a  potential
drawback to  use of SCR—are low. At the time of the
site visit,  the SCR catalyst had performed through
11,000 hours of operation including daily start-ups.(54)
Seven  larger  (370 MW to 1,000 MW) gas turbines that
employ selective catalytic reduction for NOX removal are
currently in construction or start-up phase in Japan with
no results available to date. Most, if not all, of these
units are designed for an outlet NOX concentration of 15
ppm at 15 percent oxygen.
Figure 5-3.
      Performance of Selective Catalytic Reduction
      on a Gas Turbine (54).
   . o
   u
 » o £
 C O 0.
 350

 250


 100
;
  80



  80
3
o
*
o
O
0*
z
Q.
D.
20
0



       20
 z      25

•Actual 02

 NH3/NOX = 1.03
 Ambient temp = 15C
                    50         75
                     Peak Load, %
                                   100
Data are also available on the variation of NOX reduction
with space  velocity, gas temperature, and  NH3/N03
mole ratios. These data are also for Japanese installa-
tions.
Cost data are available (54) for selective catalytic reduc-
tion units serving four large (General Electric  "Frame
6") gas turbines (total rating approximately 300 MW). In
1982  dollars the total  capital  cost would  be about
$2,650,000. The  operating cost, including all  direct and
indirect costs as well as the incremental fuel  cost, is
estimated to be  a  maximum of $0.00125 per kWh. In
order to employ  SCR, a means of cooling the exhaust
gas must be provided. The temperature range required
is from 300 to  400C  (570 to 750F), depending  on
catalyst.(53)
Efforts are underway in Japan and the United States to
develop new combustor designs  for turbines that will
reduce NOX emissions without water/steam injection or
use of  SCR.  Both catalytic combustion and staged
combustion techniques have been developed. EPA has
developed the rich-burn quick quench  (RBQQ) concept
combustor system  that uses staging to reduce both
thermal and fuel-bound NOX emissions.(55)  Testing so
far has been limited and performance data  for actual
operating units are not available.
5.3  Stationary Engines
Several methods for reducing NOX emissions from sta-
tionary engines have been employed or at least tested.
They include: water/fuel  emulsions  (diesel  engines
primarily),   exhaust gas recirculation  (diesel), lean
burning-torch ignition (spark-ignition engines only), tur-
bocharging,  charge cooling (spark),  ignition retard
(spark),  injection  retard  (diesel),  selective catalytic
reduction (spark), and  nonselective  catalytic reduction
(spark).

5.3.1   Water/Fuel Emulsion
EPA has conducted demonstration  tests on  the use of
water/fuel  emulsions to reduce  NOX  emissions from
diesel  engines.  Results for a four-stroke, six-cylinder
turbocharged diesel engine with a generator  output
rated at 165 kW are shown in Figure  5-4.(56)  NOX reduc-
tions of about 60  percent were consistently achieved
over  a wide  range of loads. The load range  also
represents a range of water-to-fuel ratios  of 0.27 to
0.60.
An important part  of  emulsion research involves in-
vestigation of the side effects of NOX reduction through
use  of water/fuel  emulsions.  Of concern  in  this
research were emissions of carbon monoxide, hydrocar-
bons, particulates, and sulfur oxides. Carbon monoxide
emissions were found to increase dramatically at low- to
mid-range loads and then to decrease to a level of about
20 percent above baseline at full load.(56) A similar ef-
fect was noticed for hydrocarbons except that at about
85 percent of load the hydrocarbon  emissions dropped
below the baseline to a value of about 60 percent of the
baseline at  full load.  Particulate  emissions  were also
higher with  NOX  control dropping  rapidly from over 2.5
                        42

-------
Figure 5-4.   NOX Reduction by Water/Fuel Emulsion for
           Diesel Engine.
   1.4





   1.2





   1.0





§  0.8

O
z



   0.6





   0.4
                                    — Baseline
                                    "••• Control effect
                                      • Catalyst
                                      • Emulsion
                                      A Combined
                              recirculation. Tests  reported for the  same engine
                              described above were carried out by water scrubbing
                              the exhaust gas from the turbocharger (to remove par-
                              ticulates) and returning a portion to mix with the incom-
                              ing combustion air.(57) The optimum value was found
                              to be about 15 percent exhaust gas by volume in the in-
                              let air, at which NOX reductions were approximately 50
                              percent. Higher reductions were obtained but the fuel
                              penalty  was excessive  and  smoke emissions  also
                              became a problem at higher proportions of exhaust gas.
                              Fuel penalty was reported in BSFC, or brake-specific
                              fuel consumption, which has units of Btu  per brake
                              horsepower-hour. Test results are shown  in Figure 5-6.

                              Data have also been collected for exhaust gas recircula-
                              tion for large-bore spark engines firing natural gas. (58)
                              Table 5-1 shows data correlating NOX emission reduc-
                              tion with the amount of exhaust gas recirculated. The
                              BSFC penalty in these tests ranged from 1 to 3 percent.

                              5.3.3  Lean-Burning Torch  Ignition
                              Another technique that has been used to reduce NOX
                              emissions from spark-ignition engines is lean-burning
                              torch ignition. Use of torch ignition extends the lean-
                              burning limit of the engine. Figure 5-7 shows test results
                              (57) for a single-cylinder, two-stroke, gas-fired engine
                              rated at 681 hp at 330 rpm. Note that the use of torch ig-
                              nition extended  the  lean-burn  limit  to  a  fuel/air
                              equivalence  ratio  of 0.55 to  0.60.  (This ratio is  the
                              percentage  of stoichiometric.) As a result, NOX emis-
                              sions can be reduced by 50  percent or  more by this
   0.2'
                            I
                40
  80
Load, kW
                                      120
                                                 160
times the baseline at zero load to less than baseline at
about 25 percent of load. At higher loads particulate
emissions stayed below the baseline level. Sulfur diox-
ide emissions were found to be essentially constant in
that they are fixed by the sulfur content of the fuel (0.24
percent  in this case).  Conversion of sulfur dioxide to
sulfate is consistently low except at zero load.

Performance data for water/fuel emulsions with diesel
engines  are also available.(57) The test engine was a
single-cylinder, four-stroke turbocharged diesel engine,
rated at 350 hp at 1,000 rpm. Water content in fuel rang-
ed from 7 to 45 percent by volume. Both high energy
and low energy emulsifiers were tested with similar
results.  Figure 5-5 shows test results  which indicate
NOX reductions  of  about  35 to  40 percent  from  a
baseline emission level of approximately 10.4 g/bhp-h
(Btu per brake horsepower-hour,  units used  for state
and local regulations for engines). Losses in  efficiency
were 4 percent or less  in these tests and increased with
water/fuel ratio.

5,3.2  Exhaust Gas Recirculation
Another method for NOX reduction that has been tested
primarily for large-bore diesel engines  is exhaust gas
                                                       Figure 5-5.   NOX Reduction by Water/Fuel Emulsion for
                                                                   Diesel Engine (57).
                                                            1.4
                                  1.2
                                  1.0
                               Z  0.8
                                ro
                               •35
                               ir
                                  0.6
                                  0.4
                                  0.2
                                                                             Emulsor
                                                              Bore,  Power, Plunger,
                                                                                        mm
                                                                                        216
                                                                                        270
                                                                                        400
O Gear pump
$Gear pump
AWesthalea^
DHomogenizer   400
•Gaulin
AGaulin
*Gaulin
 Hydroshear
                                                                                        280
                                                                                        280
                                                                                        280
                                                                                        280
                                                                     hp
350
234
234
350
                                                                            mm
24
24
20
24
                                            0.2      0.4       0.6
                                                Water/Fuel Ratio by Volume
                                                                                                0.8
                              1.0
                                                                               43

-------
Table 5-1.    NOX Reduction by Exhaust Gas  Recirculation:
            Natural Gas, Spark Ignition Engines (58)

                            % NOX Reduction
         Figure 5^7.   Effect of Lean-Burning Torch Ignition on Spark-
                     Ignition Gas-Fired Engine (57).
Approximate
% EGR
12
17
20
Pump-Scavenged
Engines
20
35
40
Blower-Scavenged
Engines
20
30
40
method. Note in  Figure  5-7 that  slight increases  in
hydrocarbon emission also result from this modifica-
tion. Factory test data are available that show an NOX
reduction of 80 percent and higher for new engines
modified to use lean-burning torch  ignition in the form
of  "jet-cell  igniters."(59)  Operation  at  fuel/air
equivalence ratios  of less  than  0.6 may affect tur-
bocharger performance somewhat because the exhaust
gas  now  has comparatively less energy  content;
however, reducing emissions to 2 g/hp-h only involves
a fuel penalty of approximately 2 percent.(58) Note  in
 Figure 5-6.   NOX Reduction by Exhaust Gas Recirculation
            for Diesel Engine (57).
                       Timing: 21,5°btdcf  1 24°btdc
  1.0
                                                            .55
                        0.60        0.65        0.70
                          Fuel/Air Equivalence Ratio, $
                                                                                                       0.76
                   8      12     16     20
                 Exhaust Gas Recirculation, %
24
                                                       Figure 5-7 that NOX emissions are given in grams per
                                                       brake horsepower-hour.
5.3.4  Charge Coo/ing
Charge cooling, sometimes  referred  to  as  charge
refrigeration, is another technique that has been applied
to spark-ignition engines, usually  on a  retrofit basis.
Test results are available for this technique as applied to
the earlier described engine.(57) Again, the NOX emis-
sions were  measured at various fuel/air equivalence
ratios but also at incoming fuel/air temperatures rang-
ing from a baseline  of  43C  (110F) down to 2C (35F).
Figure 5-8 shows the results. Note that for a given
fuel/air ratio, NOX reductions of about 40 percent were
observed  for  charge cooling to 2C  (35F).  The side
effects of charge cooling are the same as those  for
operation at leaner fuel mixtures, namely, the ignition is
further delayed and the duration of combustion is  ex-
tended. In order to combat  these conditions which
could lead to misfiring,  it may be advisable to combine
charge cooling with torch ignition or use of high energy
sparking.  Temperature  drops to less  than 5.5C (10F)
above ambient would require extensive and expensive
retrofitting including refrigeration.(60) Thus,  if such a
close temperature approach is required to meet a NOX
emission level,  this  technology would  not  be cost-
effective.
                        44

-------
Figure 5-8.   NOX Reduction by Charge Cooling for a Spark-
           Ignition Gas-Fired Engine (57).
     0.60    0.65     0.70      0.75     0.80
                 Fuel/Air Equivalence Ratio, 4
                    0.85
5.3.5  Ignition Retard
Data are available on NOX reductions in spark-ignition
engines resulting from retarding ignition timing, which
is used almost exclusively on a retrofit basis. Table 5-2
summarizes results for several types of natural gas-fired
engines.(58) Typical NOX reductions achievable range
from 15 to 30 percent. However, the fuel consumption
penalty is not negligible (up to 3 percent).

5.3.5  Turbocharg/ng
Limited data are available on the NOX reduction effect of
turbocharging a  natural gas-fired engine. (58) For tur-
bocharging to 15 in Hg,  NOX reductions were 55 percent
for pump-scavenged engines and 45 percent for blower-
scavenged  engines,  each  with aftercooling to  38C
(100F). Also,  fuel consumption decreases between 10
and 13 percent  were reported with a  corresponding
power increase of between 25 and 33 percent.
 Table 5-2.   NOX Reduction by Ignition Retard: Natural Gas-
            Fired Engines (58)
        Type of Engine
Retard, °   NOX Reduction, %
Pump-scavenged, atmospheric*
Blower-scavenged, atmospheric*
2-stroke, turbocharged
4-stroke, turbocharged,
medium pressure
4-stroke, turbocharged,
high pressure
4
4
4
5

5

15
25
30
17

25

*Not turbocharged.
5.3.7  Postcombustion Controls
In addition to during-combustion technologies for con-
trolling NOX emissions, both selective and nonselective
catalytic  reduction technologies have  been employed
for stationary engines. Most of the applications of these
after-combustion technologies have been in Japan and
in California.

Long-term (2,300 h) testing of SCR on a diesel engine
has been accomplished. The engine tested was rated at
165 kW with a displacement of 10.5 I (638 in3) and fired
No. 2 diesel fuel. The results, shown in Table 5-3, are
for extensive testing at an 80 kW load and at various
NH3/NO injection rates. Note that 90 percent reduction
(from a baseline of about 400 ppm) was achievable at
reasonable NH3 injection  rates until sometime before
2,000 hours of operation by which time catalyst perfor-
mance had declined significantly. There was, however,
significantly  improved  NOX  reduction after  catalyst
cleaning.(61) Fouling  of catalyst  by diesel particulate
was  indicated as one possible factor in catalyst deac-
tivation.

SCR has also been tested for spark-ignition engines.(57)
The engine was a six-cylinder model rated at 1,350 hp at
330 rpm and burning natural gas.  Results are shown in
Figure 5-9. Note that  reductions of 95  percent were
found over a temperature range 38C (100F) wide. With
the proper choice of  catalyst, 95 percent reduction
                           Table 5-3.
                           Cat. Hours
            NOX Reduction by Selective Catalytic Reduction
            for Diesel Engine (61)
            NO/NO Base
NH3/NO Base     NO, ppm
10-500 1.0
0.582
0.213
0.089
0.043
0.0173
0.0173
0.0173
1,000 1.0
0.586
0.471
0.371
0.214
0.143
0.077
2,000 1.0
0.635
0.541
0.486
0.446
0.378
0.292
0.243
2,300 1 .0
0.372
0.268
0.216
0.169
0.138
0.117
0.099
0
0.41
0.81
1.04
1.09
1.37
1.65
1.98
0
0.45
0.60
0.73
0.81
0.99
1.18
0
0.432
0.570
0.708
0.778
0.949
1.114
1.592
0
0.70
0.88
1.05
1.22
1.40
1.57
1.75
433
252
92
38
18.5
7.5
7.5
7.5
350
205
165
130
75
50
27
370
235
200
180
165
140
108
90
384
143
103
83
65
53
45
38
                                                                               45

-------
Figure 5-9.
    110
    100 -
NOX Reduction by Selective Catalytic Reduc-
tion for Spark-Ignition Engine (57).
Table 5-4.    Capital Costs for SCR Systems for  Lean-Burn
            Spark-Ignition Engines'* (24) (1984 dollars)
 I

 I
      400     500    600    700    800
                     Catalyst Temperature, F
                                           900    1000
could  probably be  achieved at any gas temperature
from 288C (550F) to 425C (800F). Figure 5-10 shows
results of extended tests for two catalyst-temperature
combinations.  Note that if  greater  than 80  percent
reduction is required, catalyst life may be quite limited.

The California Air Resources Board has investigated the
cost of  SCR for spark  ignition (primarily lean-burn)
engines.(42)  Table  5-4 shows some relatively recent
capital costs for several engines ranging in size from 660
to 4,000 hp. For units with manual controls for ammonia
rejection,  the  major cost  item  is catalyst;  where
automatic ammonia controls  are used, the control cost
may outweigh the catalyst cost, especially for  engines
of less than 1,000hp.

Figure 5-10.  NOX Reduction by  Selective Catalytic Reduction:
            Long-Term Test for Spark-Ignition Engine (57).
                                         20,000 h-1
                                         12.5% 02
                                         NrVNO = 1.1
Engine Size, bhp
460
820
1,280*
2,500''
5,150*
SCR Catalyst
Cost, $
29,000
47,000
71,000*
130,000*
263,000*
Cost, $
NH3 Addition Controls
Manual
6,500
7,000
7,500
8,500
11,000
Automated
50,000
51,000
52,000
54,000
59,000
                                            "Engelhard 2-stroke engines.
                                            *For 4-stroke engines, use 65% of this cost.
                                             Spark-ignition engines are also controlled by nonselec-
                                             tive catalytic  reduction  (NCR) units,  especially rich-
                                             burning engines  in  California which are required  to
                                             reduce NOX emissions by 90 percent. Table 5-5 shows
                                             data for NCR units applied to 13 rich-burn engines rang-
                                             ing from 50 to 1,100 hp and firing natural gas or, in two
                                             cases, digester gas.(62) NOX reduction efficiency after
                                             4,000 h of operation was still in excess of 80 percent on
                                             average.
                                             Costs  for NCR (in 1984 dollars), including catalyst and
                                             air/fuel controls (manual or automatic), are shown in
                                             Table 5-6.(24)
                                             Table 5-5.   NO* Reduction by NCR: Results for Tests of 13
                                                         Rich-Burn Spark-Ignition Engines (62)
No. of
Units
3
1
1
2
1
1
1
1
1
1"
Uncontrolled
Mean
404
Engine
Manufacturer
Waukesha
Waukesha
Waukesha
Waukesha
IHC
Climax
Climax
Caterpillar
Superior
Ingersoll-Rand
NOXLppmb Controlled
Std. Dev. Mean
221 36.4
Engine Characteristics
Rating, bho
83
71
51
818
50
500
300
130
500
1,100
NOX, ppm*
Std. Dev.
33.0
Loading
Cyclic
Steady
Steady
Variable
Cyclic
Variable
Variable
Steady
Steady
Steady 	
Average NOX
Reduction, %
91
                                                         "Fueled by digester gas; all others by natural gas.
                                                         bCorrected to 15% 02.
                                                          Table 5-6.    Cost of NCR Systems for Rich-Burn, Spark-
                                                                      Ignition Engines" (62) (1984 dollars)
                                                                                    Air/Fuel Controls
                                                          Engine Size  NSCR Catalyst         Cost, $	   Dual or
                        40       60
                        Elapsed Time, h
                                                    100
bhp
70
280
585
1,170
Cost, $
2,000
6,200
11,400
19,700
Manual
1,300
1,300
2,000
2,000
Automatic
7,900
7,900
10,900
10,900
Single
Single
Single
Dual
Dual
                                              "Engelhard Systems.
                          46

-------
                                             Chapter 6
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                                                 47

-------
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                       48

-------
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62. Rawuka, A. NOX Reduction Program for Gas Fueled
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