£EPA
United States      Environmental Monitoring Systems EPA/600/4-85/047
Environmental Protection  Laboratory         July 1985
Agency        Research Triangle Park NC 27711
Research and Development
Asbestos-Containing
Materials in School
Buildings:

Bulk Sample Analysis
Quality Assurance
Program—Bulk
Sample Rounds 9, 10,
11 and Blind Round II

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                                      EPA/600/4-85/047
                                      July 1985
        ASBESTOS-CONTAINING MATERIALS
      IN SCHOOL BUILDINGS:   BULK SAMPLE
     ANALYSIS QUALITY ASSURANCE PROGRAM

      Bulk Sample Rounds 9, 10, 11 and
               Blind Round  II
                     by
  D. A. Pasquini, M. L. Parris,  L.  T.  Laird
         Research Triangle Institute
Research Triangle Park, North Carolina  27709
           Contract No. 68-02-3767


     Project Officer:  Michael  E.  Beard
         Quality Assurance Division
 Environmental Monitoring System Laboratory
    U.S. Environmental  Protection Agency
     Research Triangle Park, N.C.  27711

        .Exposure Evaluation Division
         Office of Toxic Substances
  Office of Pesticides  and Toxic Substances
    U.S. Environmental  Protection Agency
           Washington,  D.C.  20460

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                              Disclaimer

     The information in this document has been funded wholly or  in part
by  the  United  States  Environmental  Protection  Agency  under  contract
#68-02-3767 to the Quality Assurance Division, Environmental Monitoring
Systems Laboratory,  Research Triangle  Park,  North  Carolina.    It has
been subject to the agency's peer and administrative review, and it has
been approved  for publication as  an EPA document.   Mention  of  trade
names  or  commercial  products  does  not  constitute  endorsement  or
recommendation for use.
                                 ii

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                           TABLE OF CONTENTS
Section                                                           Page

Abstract	    11

Tables 	     v

1.0  Introduction	   1-1
2.0  Procedures and Methods	   2-1
     2.1  Bulk Sample Rounds	   2-1
          2.1.1  Bulk Sample Repository.  . .	   2-1
          2.1.2  Selection of the Bulk Material Samples	   2-1
          2.1.3  Reference Analysis of the Bulk Material
                 Samples	   2-1
          2.1.4  Distribution of the Bulk Material Samples
                 to the Participating Laboratories 	   2-2
          2.1.5  Laboratory Performance Reports	   2-3
     2.2  Blind Round	   2-3
          2.2.1  Introduction	   2-3
          2.2.2  Procedures and Methods	   2-4
3.0  Results and Discussion	   3-1
     3.1  Bulk Sample Round 9	   3-1
     3.2  Bulk Sample Round 10	   3-4
     3.3  Bulk Sample Round 11	   3-6
     3.4  Blind Round II	   3-5
4.0  Summary	   4-1
Appendix A:  Reporting Form, Coding Form, and  Instructions  .  .  .   A-l
Appendix B:  Report to Laboratories  	   B-l
Appendix C:  Interim Listing*Number 18  	   C-l
Appendix D:  Quantitative Results   	   D-l
                              in

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                               ABSTRACT
     This report  presents  the  results of laboratories participating  in
the ninth, tenth, eleventh and second  blind  round(s)  of  the  bulk  sample
analysis quality  assurance program  sponsored  by  the U.S.   Environmental
Protection   Agency.     Two  hundred   fifty-four,  320,   318  and   50
laboratories which  analyze bulk  samples  for  determination  of  asbestos
content  by   polarized  light microscopy  participated  in  these  rounds,
respectively.
     Laboratories received  bulk  samples  of  asbestos, asbestos  substi-
tutes or other  bulk  insulation materials.  Three aspects  of analytical
results are  considered:   classification  of a sample  as either  asbestos
(positive)  or  nonasbestos  (negative);  identification of  the  specific
type of asbestos  present, and quantisation of the relative amount  of
major  constituents  present.   A  performance  rating  was  made for  each
laboratory,   based only on  the ability to correctly  classify  samples.
Reductions of  all correct (4/4 or  3/3)  scores  were  made  only for  the
reporting of false positives and false negatives.  Laboratories partic-
ipating in rounds 9, 10, 11 and the second blind  round correctly  class-
ified 92.1%, 97.2%,  94.9% and 97.9% of the samples, respectively,  as  an
asbestos or  nonasbestos containing  material as described  in  the Federal
Register, Vol. 47, No. 103, Thursday, May  27, 1982.
     Continuation of  the  program  is  anticipated.    Any  commercial  or
noncommercial  laboratories with  capability  in   polarized  light micro-
scope analysis  of bulk  samples may  participate.   Results  of commercial
laboratories are  published  in  the  interim listing of "Commercial  Labo-
ratories with Polarized Light Microscope  Capabilities for  Bulk  Asbestos
Identification."
     This  report  is  submitted  in   fulfillment  of contract   number
68-02-3767 by Research Triangle  Institute under  the  sponsorship of  the
U.S. Environmental Protection Agency.  This report covers  a  period from
January 1, 1984 to December 31,  1984  and work was completed  as of June
30, 1985.
                                 IV

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                                TABLES
Number                                                          Page
   1      Listing of Commercial  Laboratories Participating
          in Blind Round II                                      2-4
   2      Commercial Laboratory Listing  by  EPA  Region            2-7
   3      Round 9 Qualitative Results                            3-2
   4      Round 9 Performance Ratings                            3-4
   5      Round 10 Qualitative Results                           3-5
   6      Round 10 Performance Ratings                           3-6
   7      Round 11 Qualitative Results                           3-8
   8      Round 11 Performance Ratings                           3-9
   9      Blind Round II Qualitative Results                     3-11
  10      Blind Round II Quantitative Results                    3-12
  11      Blind Round II Performance Results                     3-13

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                               SECTION 1
                             INTRODUCTION

     The U.S. Environmental Protection Agency (EPA) Asbestos-in-Schools
Program designated polarized light  microscopy  (PLM),  supplemented when
necessary by x-ray powder diffraction,  as  the recommended  method for
detecting  asbestos  in  friable   materials.l>2     in  January  1980,  a
quality assurance  (QA) program  was  initiated  for  laboratories  having
capability  in PLM  analysis of  bulk  samples.  The  goals  of the program
were twofold:  first,  to assist  laboratories in developing reliable PLM
analytical  capability  by providing an independent check on data quality
and by supplying characterized samples for use in internal quality con-
trol; and,  second, to  facilitate public  access  to competent analytical
laboratories.   Commercial  or  noncommercial   laboratories  with  PLM ana-
lytical capabilities are eligible to participate in the EPA-QA program.
Participation in this  inter!aboratory testing  program does not lead to
accreditation,  certification,  endorsement  or  other  official  approval
for bulk asbestos sample analysis.
     Participating commercial  laboratories   and their performance rat-
ings  are  listed   in   a  written  report   Commercial   Laboratories  with
Polarized Light  Microscope Capabilities for Bulk  Asbestos  Identifica-
tion,  Interim Listing  Number  XX, EPA  Bulk  Asbestos  Round  XX  and made
available after  each  QA round  to EPA regional  asbestos coordinators,
state  asbestos  contacts,  and  the general public.   Further  information
on the  QA  program,  participating laboratories,  and/or  procedures for
sampling and  analysis  of asbestos-containing bulk  materials is  avail-
able by contacting the Program Technical  Information  Service using the
toll-free number 1-800-334-8571,  extension 6741.

1  CfrR» Title  40, Subpart F.    Friable  Asbestos-Containing Materials
   in schools.  Section 763.109, Analyzing Friable Material.
2  Test Method  -  Interim Method  for  the Determination  of  Asbestos in
   Bulk  Insulation  Samples,U.S.EnvironmentalProtectionAgency,
   PublicationNumber  EPA-600/M4-82-020,   Environmental   Monitoring
   Systems Laboratory, Research Triangle Park,  North Carolina, December
   1982.
                                  1-1

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   Rounds 1  and  2  of the QA Program were  conducted in 1980.   Results
were reported in two  EPA reports:   published in August  1980,  EPA-560/
13-80-23, EPA-560/5-81-001, and published  in March  1981.   Rounds  3 and
4  were  conducted  in June  1981 and  January  1982, respectively,  and
results were reported in  an RTI  report  (Contract  Number  68-02-3431)  in
June 1982.   The  results of Rounds 5, 6,  7,  8,  and Blind  Round  I  were
reported  in  an  RTI  report  (Contract  Number 68-02-3431)  in  February
1985.  This report describes the results of Rounds 9,  10,  11, and Blind
Round II.
                                   1-2

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                               SECTION 2
                        PROCEDURES  AND METHODS

     This  section  reviews the procedures  and methods  followed in  con-
ducting  the QA bulk  sample and blind rounds.  Section 2.1 discusses  the
selection  and distribution of the bulk samples, the reporting  forms  and
laboratory instructions,  the bulk sample reference reports, the labora-
tory  reports,  and  the   calculation  of  the laboratory's  performance
rating in  Bulk Sample Rounds 9,  10, and  11.   Section 2.2 discusses  the
selection  of  laboratories and  analysis  of  the  laboratory  results  in
Blind Round II.
2.1  BULK  SAMPLE ROUNDS
2.1.1  Bulk Sample Repository
     Bulk  sample  materials  are  stored  in  a   repository  located   at
Research Triangle  Institute  in Research  Triangle  Park,  North  Carolina.
The repository contains  laboratory  formulated  asbestos  and nonasbestos
materials,  real-world  materials  supplied by  asbestos  removal  contrac-
tors and manufacturers,  and  fibrous asbestos substitutes that  are pur-
chased or  provided by manufacturers.  Industrial  samples are taken from
the bulk materials  in  the repository  and  packaged in  plastic bags  or
plastic vials.
2.1.2  Selection of the Bulk Material Samples
     When  a bulk material is selected  for distribution  in  a QA round,
it is analyzed in  the RTI Optical Microscopy Laboratory for uniformity
and asbestos content.  The results  of this  analysis  are compared with
results of the screening  analysis performed on the  bulk material when
it was first received at  the RTI  repository.  If the two analyses agree
in terms  of asbestos  content  and  consistency,  a sample  of  the bulk
material  is sent  to the reference laboratory for characterization.
2.1.3   Reference  Analysis of the  Bulk Material  Samples
     Reference analysis of the bulk material samples are  performed by
the Bureau  of Mines, U.S. Department of the Interior,  Avondale,  Mary-
land.   The bulk sample is  analyzed  for asbestos content using  PLM and,
if the analyst deems it necessary, x-ray powder  diffraction.
                                  2-1

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     The bulk  sample  is  first  examined with a low power  (approximately
10-45X) stereo  binocular microscope for  gross  characterization.   From
two to eight slides are  then prepared  for PLM examination using materi-
al taken from different  positions of each sample or each  layer within  a
sample.  Examination  is  done at magnification ranging from approximate-
ly 40X to 400X with most characterization being done at low  power.
     The number  of  slides  prepared and  examined  are  determined by  the
analyst's experience  and his  judgement of the component complexity  and
homogeneity of each sample  or  layer.   The  area  percent of   asbestos is
visually estimated with  the aid  of  modal  percentage charts   and this is
converted to an  estimated weight  percent based  on the  analyst's exper-
ience with  similar  materials.   Other  fibrous nonasbestos materials in
the bulk sample  are estimated  by  weight  percent  in the same manner  and
listed in the analysis report.  When a bulk sample contains  two or more
layers, each layer  is weighted according to its thickness to calculate
the total estimated weight  percentage  of the components for the entire
bulk sample.
     If the results of the reference analysis agree with  the RTI analy-
sis for a given  bulk  material  sample,  it is then confirmed  for distri-
bution in the QA round.  Characteristics  on which agreement  between  the
reference  analysis  and  the   RTI  analysis  must  be   reached  include:
classification  of  the bulk  sample  as  an asbestos containing  or non-
asbestos containing  material,  agreement on  the type  of  asbestos  if
asbestos is  present  and general  agreement  on  the composition  of  the
major components of the  sample.
2.1.4  Distribution of the Bulk Material  Samples to the Participating
       Laboratories
     Usually a set of four different bulk materials is  sent  to the par-
ticipating laboratories  in a given  bulk material round.   Each bulk sam-
ple is individually packaged in a sample  vial or plastic  bag, placed in
another  plastic  bag,   and  then inserted  into a  padded envelope  along
with  reporting and  coding  forms,  and  analysis  instructions.   Labora-
tories  are  given 20  working  days following  sample  receipt  to analyze
the set of bulk  material samples  and to  return their analytical results
to RTI.
                                   2-2

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     The reporting form, coding  form,  and  instructions  that are used by
the  participating laboratory  to  process  and  record their  analytical
results are included  in Appendix A.  The  reporting form includes a data
entry  space  for the  identification  of asbestos fibers  and  nonasbestos
materials, analytical method(s)  used,  quantitative procedures used,  and
quality  control  measures  employed.   The  coding  form  summarizes  the
information on  the reporting form  and  is  used  by RTI  to record a labor-
atory's analytical results.
2.1.5  Laboratory Performance Reports
     Laboratory  performance  is  based on the ability  of  a  laboratory to
determine  if  a bulk  material  sample does or  does not  contain  greater
than 1 percent  asbestos.   A performance  rating is calculated  based on
the number of  classification errors made by the  laboratory.   A classi-
fication error can either  be  a false  positive (nonasbestos)  or  false
negative (no  asbestos reported  in a  sample  containing greater than  1
percent asbestos).
     A written  report is  sent to  each participating laboratory at  the
completion  of  each  round   (see  Appendix  B).    This   report  lists  the
qualitative results of the Bureau  of Mine's  reference analysis  for each
bulk  sample,  the  participating  laboratory's   performance  rating,  the
number of  false negatives  and/or positives reported  by  the  participat-
ing  laboratory, and  a  cumulative  distribution for  the percentage  of
asbestos reported in  each  bulk  sample by  the participating  laborato-
ries.  Identification errors,  resulting from the  incorrect  identifica-
tion of a mineral  species  is also indicated on the report  to laborato-
ries.  Identification errors do  not result in  a  reduction  of a labora-
tory's performance rating.
2.2  BLIND ROUND
2.2.1  Introduction
     Great time and   effort  is  assumed to  be   taken  by the  commercial
laboratories  in  their analyses  of bulk material  QA samples.   The  pur-
pose of the blind round is to determine to what extent  the  same results
can be expected  in terms of  analytical accuracy and  precision  in  their
analyses of non-EPA bulk samples.
                                  2-3

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     The EPA instructed RTI to prepare a separate set of bulk materials

for analysis by a group of randomly selected commercial  laboratories.

2.2.2  Procedures and Methods
     The  laboratories  participating  in the  second  blind   round  were
randomly selected from  those  listed in the RTI  publication  Commercial
Laboratories  with  Polarized  Light  Microscopy   Capabilities  for  Bulk
Asbestos Identification,  Interim  Listing  Number 15,  EPA  Bulk  Analysis

Round 8.
     Altogether 50 commercial  laboratories  participated  in  the  second

blind round.  Table  1 lists  these  50  laboratories  and their  geographi-
cal location.
   TABLE 1.  LISTING OF THE COMMERCIAL LABORATORIES PARTICIPATING IN
             BLIND ROUND II
  Region
 Laboratory name
 Laboratory location
    II
   III
Aetna Insurance Company
State of Connecticut
ESA
LBH Associates
Hartford Fire Insurance
Tibbetts Engineering Corporation

Atlantic Environmental, Inc.
Alternative Ways, Inc.
Kaselaan & D'Angelo Associates, Inc.
Princeton Testing Laboratory
Inter-City Testing Laboratory
IHI-Div. Kemron
Enviro-Probe, Inc.

Tracor-Jitco, Inc.
Lancaster Laboratories, Inc.
Microbac, Inc.
Pittsburgh Testing Labs
Commonwealth Laboratory, Inc,
Industrial Hygiene & Occup. Med. Lab
Hartford, CT
Hartford, CT
Bedford, MA
Newton, MA
Hartford, CT
New Bedford, MA

Montville, NJ
Willingboro, NJ
Haddon Heights, NJ
Princeton, NJ
Mineola, NY
Huntington, NY
Bronx, NY

Rockville, MD
Lancaster, PA
Erie, PA
Pittsburgh, PA
Richmond, VA
Fairfax, VA
                                  2-4

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                       TABLE  1.   (continued)
Region
 Laboratory name
 Laboratory location
  IV
  VI



 VII


VIII

  IX
Tuscaloosa Testing Laboratory, Inc.
Applied Technology Consultants
Southern Research Institute
Thompson Engineering Testing
Geo-Enviromental Services, Inc.
Law Engineering Testing Co.
McCrone Environmental Services
McCoy and McCoy, Inc.
Environmental Protection Systems,
  Inc.
Micro-Methods

CENCON
Gabriel Laboratories, Ltd.
Randolph and Associates
MJH Mineralogical Consulting, Inc.
Analytical Consulting Testing
Herron Testing Laboratories
Bowser-Morner Testing Laboratories,
  Inc.
A & G Microscopy

Intox Laboratories, Inc.
Albuchemist, Inc.
Southwestern Laboratories, Inc.

Baird Scientific
Larron Laboratory

Mountain Analysts Corp.

Contaminant Analysis Services, Inc.
Fireman's Fund Insurance Co.
Finkel Analytical Laboratory
Health Science Associates
C.E.D., Inc.
Casalina Associates, Inc.

Microlab Northwest
Tuscaloosa, AL
Opelika, AL
Birmingham, AL
Mobile, AL
Atlanta, GA
Atlanta, GA
Norcross, GA
Madisonville, KY
Jackson, MS

Pascagoula, MS

Chicago, IL
Chicago, IL
Peoria, IL
Apple Valley, MN
Cuyahoga Falls, OH
Cleveland, OH
Dayton, OH

Arlington, WI

Redfield, AR
Albuquerque, NM
Dallas, TX

Carthage, MO
Cape Giradeau, MO

Denver, CO

Tucson, AZ
Petaluma, CA
Long Beach, CA
Los Alamitos, CA
Pinole, CA
Kaneohe, HI

Redman, WA
                               2-5

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below:
     The  laboratory  selection   process  followed  the  steps  outlined
     1.  All of the commercial laboratories participating in Round 8 of
         the U.S. EPA's Bulk  Asbestos  Sample  Quality  Assurance Program
         were grouped by EPA  Region  (1 through  10).   Table  2 lists the
         number of commercial laboratories by EPA region.

     2.  Fifty laboratories or approximatley 30 percent of the 169 com-
         mercial  laboratories listed in  Interim Listing  Number 15, EPA
         Bulk  Analysis  Round 8  were  selected  to  participate  in the
         second blind  round.   The number  of  laboratories  selected per
         EPA  region   corresponds  to  the  proportionate  percentage  of
         laboratories  located in  a  given  EPA  region.   For  example,
         Region 1 contained  20 (or  11.8  percent)  of the 169 commercial
         laboratories that  participated  in Round 8 of the  Bulk Sample
         Asbestos Quality  Assurance  Program.   Therefore, Region  I was
         allocated 6  (or approximately 12.0  percent)  of  the 50 commer-
         cial laboratories stated for the  second blind round.  Based on
         this  type  of rationale,  the  laboratory allocations  for each
         EPA region were determined, as given in Table 2.

     3.  Each commercial laboratory  that  participates  in  the Bulk Sam-
         ple  Asbestos Quality Assurance  Program  is  assigned  a  four-
         digit identification number as explained below:

         0  The first digit  corresponds  to the  EPA region (1 through 9
            for Regions 1 through 9, and 0 for Region 10)

         0  The second digit  corresponds to the State (number 1 through
            9 depending on  the number  of States located in the Region)
            where the laboratory  is  located.

         0  The last  two digits  are  a  computer-assigned  random number.
            A  laboratory was selected  for the  second  blind  round when
            its computer-assigned random  number matched  the two-digit
            random  number  manually  extracted   from  a  random  number
            table.

     4.  A  commercial  laboratory selected  for  the second  blind  round
         was  replaced with another commercial laboratory located in the
         same EPA region when the originally  selected laboratory

         0  Did not accept samples for asbestos analysis,

         0  Accepted  bulk  samples for  asbestos  analysis  only from com-
            mercial clients,

         0  Did not respond  to the surveyor's request for information,

         0  Had ceased operations,

         0  Requested  an analysis fee  greater than $150 for three bulk
            asbestos  samples, and/or

         0  Recommended  or  referred the  caller to  another commercial
            laboratory.

                                  2-6

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               TABLE 2.  COMMERCIAL LABORATORY LISTING BY EPA REGION, AS GIVEN IN INTERIM LISTING,
                         NUMBER 15, COMMERCIAL LABORATORIES WITH POLARIZED LIGHT MICROSCOPE
                         CAPABILITIES FOR BULK ASBESTOS IDENTIFICATION, MARCH 1984
ro
i
EPA
Region
I
II
III
IV
States in
EPA region
Connecticut
Maine
Massachusetts
New Hampshire
Rhode Island
Vermont
New Jersey
New York
Delaware
Maryl and
Pennsylvania
Virginia
West Virginia
District of Columbia
Alabama
Florida
Georgia
Kentucky
Mississippi
North Carolina
South Carolina
Tennessee
Number of
commercial
laboratories
located in region
20
23
21
33
Percentage
of commercial
laboratories
located per region
11.8
13.6
12.4
19.5
Number of commercial
laboratories surveyed
per region
6
7
6
10

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                                                    TABLE 2.  (continued)
ro
oc

EPA
Region

V





VI




VII



VIII






States in
EPA region

Illinois
Indiana
Michigan
Minnesota
Ohio
Wisconsin
Arkansas
Louisiana
New Mexico
Oklahoma
Texas
Iowa
Kansas
Missouri
Nebraska
Colorado
Montana
North Dakota
South Dakota
Utah
Wyoming
Number of
commercial
laboratories
located in region
26





10




7



4





Percentage
of commercial
laboratories
located per region
15.4





5.9




4.1



2.4





Number of commercial
laboratories surveyed
per region

8





3




2



1






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                                                    TABLE 2.  (continued)
1C
EPA
Region
IX
X

States in
EPA region
Arizona
California
Hawaii
Nevada
Alaska
Idaho
Oregon
Washington
TOTAL
Number of
commercial
laboratories
located in region
20
5
169
Percentage
of commercial
laboratories
located per region
11.8
3.0
99.9
Number of commercial
laboratories surveyed
per region
6
1
50

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                               SECTION 3
                        RESULTS AND DISCUSSION

     The results of  Bulk  Sample Rounds 9, 10,  11,  and Blind Round  II
are described in this section.   The total  number of laboratories parti-
cipating in each round  is listed  in  the introductory  paragraph  of each
round along with-a summary of  the laboratory's  analytical  results.   In
addition, a description of the bulk material  samples used in each round
is provided.
3.1  BULK SAMPLE ROUND 9
     Round 9  samples were distributed  on April 27,  1984.    Four bulk
samples  were  sent  to  a total   of 254  participating  laboratories (176
commercial and 78 noncommercial).  Quantitative results  were available
for 237 laboratories (170 commercial  and 67 noncommercial).
     Samples A and  B were prepared for evaluation of quantitative esti-
mates  provided  by  participating  laboratories.   Samples  C and  D were
obtained from removal projects.  Sample A contained 1.8 to 2.0 grams of
a  mineral  wool/calcium  carbonate mixture and  8 to  12  milligrams  of
mine-grade chrysotile.   It was estimated  to  contain 0.40  to  0.66 per-
cent asbestos, by weight.  Sample B  contained 1.8  to  2.0  grams  of  the
same mineral wool and  calcium  carbonate mixture used  in  sample  A with
90 to 110 milligrams of mine-grade amosite.   Sample 8  was estimated to
contain 4 to 6 percent asbestos, by weight.  Sample C  contained  chryso-
tile,  fibrous  gypsum,  vermiculite,  and calcium carbonate.   Sample  D
contained fibrous glass, cellulose, and calcium carbonate.
     The qualitative results  for Round  9  are  presented in  Table  3.   Of
the 948 samples  analyzed  in  Round 9, 873  (92  percent) were classified
correctly  while  848. (89  percent)   were  classified  and  identified
correctly.
     .Sample A contained  less  than 1  percent  of chrysotile,  by  weight.
As a  result  of the  various  analytical  techniques utilized  during  PLM
quantitative procedures, 39 of the 237 laboratories (16  percent) that
analyzed sample A in Round 9  reported an asbestos concentration  between
                                  3-1

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                                          TABLE  3.    ROUND  9 QUALITATIVE RESULTS
Sample
ID
A




B




C



D




Sample
contents
Chrvsotile, 90%
TOTAL
Number of
samples
analyzed
237




237




237



237



948
Number of
correct
classifications
186 (78.5%)




218 (92.0%)




237 (100.0%)



232 (97.9%)



873 (92.1%)
Number of
classification errorsb
False
Negatives
0




19




0



0



19
False
positives
51




0




0



5



56
Number of
identifi-
cation
errors c
5




15




5



0



25
Total number
correctly
classified anc
identified
181 (97.3%)




203 (85.7%)




232 (97.9%)



232 (97.9%)



848 (89.5%)
CO
I
ro
       3 Correctly  classified  as  an  "asbestos  containing material"  as  described  in  the Federal  Register/Vol.  47,
        No.  103/Thursday,  May 27, 1982/Rules  and  Regulations/pg.  23370/Section  763.103,  Definitions.

       b Samples may be  classified as  asbestos-containing  (positive) or  as  nonasbestos (negative).   Classifica-
        tion errors are false positives  or  false  negatives.

       c Identification  errors are incorrect designations  of  the  specific type(s)  of asbestos present.   Identifi-
        cation and classsfication errors are  mutually  exclusive  categories;  i.e.,  incorrect classifications  are
        not  counted as  identification errors.

-------
one  and five  percent  and 12  laboratories  (5  percent)  reported  an
asbestos concentration of  greater  than  5  percent.  Of  the  237  labora-
tories that analyzed sample A in Round 9,  186  (78 percent)  reported an
asbestos concentration of 1 percent or less.
     Considering  the  variations in  analytical  procedure, EPA  decided
that although 186  (78 percent)  of  the 237  laboratories  correctly clas-
sified sample A as containing less than  one percent asbestos by weight,
it would not reduce the  remaining  51  (22  percent) laboratories  perfor-
mance ratings.   Therefore, a laboratory reporting  an  asbestos  content
of 5 percent or less was given  credit for  sample  A.   This allowance to
5 percent  was  misinterpreted by  some participating  laboratories  that
EPA had changed it's definition of an asbestos containing material  (any
material which  contains  more than 1  percent of  asbestos,  by weight).
In  fact,   the   EPA 1  percent  definition  of   an asbestos  containing
material had not been changed.
     Because of  this  misunderstanding EPA  elected  to remove sample  A
from Round 9.  Round 9 is recorded as having only 3 samples, samples B,
C, and D.   The maximum performance rating for Round 9 is 3/3, depending
on your score for  samples B, C, and D.
     Sample C was  commonly misidentified as containing tremolite.  How-
ever, as noted  in  section  2.1.5,  identification errors  are  not  counted
against the  laboratories'   performance  ratings.   The  distribution  of
quantitative results  for  participating  laboratories  is presented  by
sample  in  Appendix D,  Figures 1  through  4.   Results  are  mailed  to
participating laboratories for  interlaboratory comparison.
     The distribution of performance ratings for Round  9 is presented
in Table  4.    Of  the 237  participating laboratories  in Round   9,  191
received a performance  rating of 3/3 (no  classification errors),  39  a
performance rating of 2/3 (one  classification error), 6 received a per-
formance rating  of 1/3,   and 1 received  a performance  rating  of  0/3.
                                  3-3

-------
                 TABLE 4.   ROUND  9  PERFORMANCE  RATINGS
Performance
rating
3/3
2/3
1/3
0/3

Classification
errors
0
1
2
3

Number of
identification errors
0 1 2
179
30
4
1
214
11
8
2
_0
21
1
1
0
£
2
Number of
laboratories
191 (80.6%)
39 (16.5%)
6 (2.5%)
_1 (0.4%)
237
3.2  BULK SAMPLE ROUND 10
     Round 10 samples were distributed on September 7,  1984.   Four sam-
ples were sent  to  a  total  of 320 participating  laboratories  (223 com-
mercial  and  97  noncommercial).   Results  were  returned by 282  labora-
tories (197 commercial and 85 noncommercial).
     All of  the bulk  materials distributed  in Round  10 were  real-world
samples.  Sample A contained chrysotile  (8  - 13  percent),  perlite,  and
gypsum.  Sample B contained  chrysotile (50  - 60  percent)  and  cellulose
fibers.  Sample C  contained cellulose,  and Sample D contained  fibrous
glass with small amounts of mica and  carbonate.  Neither  sample  C or D
contained asbestos.
     The qualitative results for Round 10 are presented in Table 5.   Of
the 1,128 samples  returned  in  Round 10,  1,096 (97 percent) were clas-
sified correctly while  1,082 (96 percent) were  classified and  identi-
fied correctly.
                                  3-4

-------
                                            TABLE  5.   ROUND  10  QUALITATIVE  RESULTS
Sample
ID
A
B
C
D

Sampl e
contents
Chrysotile, 8-13%
Gypsum, 50-60%
Perlite, 30-40%
Chrysotile, 50-60%
Cellulose, 40-50%
Cellulose, >99%
Gypsum, <1%
Quartz, <1%
Fibrous glass, >97*
Mica & carbonate,
TOTAL
Number of
samples
analyzed
282
282
282
282

1128
Number of
correct
classificationsa
261 (92.6%)
280 (99.3%)
274 (97.2%)
281 (99.6%)

1096 (97.2%)
Number of
classification errors'5
False
negatives
21
2
0
0

23
False
positives
0
0
8
1
9
Number of
identifi-
cation
errorsc
8
6
0
0

14
Total number
correctly
classified and
identified
253 (89.7%)
274 (97.2%)
274 (97.2%)
281 (99.6%)

1082 (95.9%)
CO

(Jl
          a Correctly  classified  as  an  "asbestos containing  material"  as  described  in the Federal  Register/Vol.  47,
           No.  103/Thursday,  May 27, 1982/Rules and Regulations/pg.  23370/Section  763.103,  Definitions.

          " Samples may be  classified as  asbestos-containing (positive) or  as  nonasbestos (negative).   Classifica-
           tion errors  are false positives or false negatives.

          c Identification  errors are incorrect designations of  the  specific  type(s)  of asbestos present.  Identifi-
           cation and classification errors  are mutually  exclusive  categories;  i.e., incorrect classifications  are
           not  counted  as  identification errors.

-------
     The  distribution  of  quantitative results  for the  participating
laboratories  is  presented by  sample  in Appendix  D,  Figure 5  through
8.   This  information is supplied to  the participating  laboratories  to
enable them to compare their quantitative results with  those of others.
Again, quantitative  results are  not used in  determining  a laboratory's
performance rating.
     The distribution of  performance  ratings for Round 10 is  presented
in Table 5.  Out of the 282 laboratories participating  in Round 10, 253
received  a performance rating  of  4/4  (no  classification  errors),  26
received  a performance  rating of 3/4  (1  classification  error),  and  3
laboratories received a  performance rating  of 2/4  (two  classification
errors).   The  laboratories  scoring 4/4 recorded   six  single  and two
double identification errors,  and the  laboratories  scoring 3/4  recorded
three single identification errors.   Of the  three  laboratories scoring
2/4, only one made a single identification  error.

                TABLE 6.  ROUND 10  PERFORMANCE  RATINGS

Performance
rating

4/4
3/4
2/4

Number of
classification
errors

0
1
2

Number of
identification
errors
0 1 2
245
23
2
270
6
3
1
10
2
0
0
2

Number of
laboratories

253 (89.7%)
26 (9.2%)
3 (1.1%)
282
3.3  BULK SAMPLE ROUND 11
     Round 11 samples were distributed on November 12,  1984.   Four bulk
samples  were  sent to  a  total of  318 participating laboratories  (224
commercial and 94 noncommercial laboratories).   Laboratory reports were
returned by a total of 278  laboratories  (198 commercial  and 80  noncom-
mercial) .
                                  3-6

-------
     Sample A  contained 100 percent  fibrous  glass that  had  been  dyed
red.    Sample  B  contained  approximately 98  percent mine-grade crocido-
lite with 2 percent  opaque  complementary minerals.   Sample C contained
>98 percent pyrophyllite and <2 percent  lime.   Pyrophyllite is used in
refractories,  asphalt fillers, joint compounds, paints, roofing materi-
als, and  wallboard.   Sample D was  100  percent carbon  fibers.   Carbon
fibers  are being used with increasing frequency to strengthen materials
as production  costs come down and applications increase.
     Sample C  was  selected because  it  is easily confused  with  antho-
phyllite  or tremolite-actinolite  asbestos.   The  refractive  indices of
pyrophyllite are lower and the birefringence is higher than correspond-
ing properties of anthophyllite or tremolite-actinolite.
     The  qualitative results for Round 11 are presented in Table 7.  Of
the 1,112 samples returned in Round 11,  1,055 (95 percent) were classi-
fied correctly while 1,041  (94 percent)  were  classified and identified
correctly.
     There were five classification errors of Sample A, which is attri-
buted to  the laboratories  indicating  that chrysotile  was  present.   The
three classification errors in sample B  indicated that the sample  con-
tained  either  fiberglass  or  was   listed  as  being   "other"  material.
Sample  C  was commonly  classified  as containing  actinolite,  anthophyl-
lite, or tremolite and, to a lesser extent,  chrysotile.  The laboratory
misclassifying carbon fibers, indicated  that  the  sample contained  cro-
cidolite.
     The 14 identification errors recorded for  sample B indicated  pri-
marily  amosite to be present rather  than mine-grade  crocidolite.   To a
lesser  extent,  laboratories  indicated that  unspecified materials  were
present.  One  laboratory indicated chrysotile to be present.
     Quantitative results for participating  laboratories  are presented
in Appendix D, Figures 9 through  12.   This information  is  provided to
participating  laboratories  for  interlaboratory  comparison  although
these data are not used in determining performance ratings.
                                  3-7

-------
                                              TABLE  7.  ROUND  11  QUALITATIVE  RESULTS
Sample
ID
A
B
C
D
Sample
contents
Fibrous glass, 100%
Crocidolite, >98%
Opaques, carbonates,
and trace unidenti-
fied phases, <2%
Pyrophyllite, >98%
Lime, <2%
Carbon fibers, 100%
TOTAL
Number of
samples
analyzed
278
278
278
278
1112
Number of
correct
classifications3
273 (98.2%)
275 (98.9%)
230 (82.7%)
277 (99.6%)
1055 (94.9%)
Number of
classification errors^
False
negatives
0
3
0
0
3
False
positives
5
0
48
1
54
Number of
identifi-
cation
errors0
0
14
0
0
14
Total number
correctly
classified and
identified
273 (98.2%)
261 (93.9%)
230 (82.7%)
277 (99.6%)
1041 (S&rT*)
U)
I
CO
          a Correctly classified as an "asbestos containing material" as described in the  Federal Register/Vol.  47,
            No. 103/Thursday, May 27, 1982/Rules and Regulations/pg. 23370/Section 763.103,  Definitions.

          b Samples may be classified as asbestos-containing (positive) or as nonasbestos  (negative).   Classifica-
            tion errors are false positives or false negatives.

          c Identification errors are incorrect designations of the specific type(s) of asbestos present.   Identifi-
            cation and classification errors are mutually exclusive categories; i.e., incorrect classifications  are
            not counted as identification errors.

-------
     The distribution of  the  performance ratings for Round 11  is pre-
sented in Table 8.  Of the  278  laboratories  participating  in  Round 11,
223 received a performance rating of 4/4 (no classification errors), 53
received a performance rating of 3/4 (one classification error), (and 2
received a performance rating of 2/4.

                TABLE 8.  ROUND 11 PERFORMANCE RATINGS
Performance
rating
4/4
3/4
2/4

Number of
classification
errors
0
1
2

Number of
identification
errors
0 1 2
213
49
2
264
10
4
_0
14
0
0
£
0
Number of
laboratories
223 (80.2%)
53 (19.1%)
2 (0.7%)
278
 3.4   BLIND  ROUND  II
      Three  bulk  asbestos  samples  were sent to  each  of the  commercial
 laboratories  participating  in  the  second blind  round.   Sample A  con-
 tained  mixed  amosite and  chrysotile  (80  percent).  Sample  B  contained
 layered amosite  and  chrysotile  (>95 percent).   Sample  C contained  mixed
 cellulose,  graphite fibers,  vermiculite.   The  bulk  materials  used  in
 Samples A,  B,  and C  were furnace insulation,  ceiling  material, and pipe
 insulation, respectively.  Each material  was  previously used  as a bulk
 material  sample  in the U.S.  Environmental   Protection  Agency's  Bulk
 Asbestos  Sample  Quality Assurance Program.
                                  3-9

-------
     A  laboratory's  analytical  results were  evaluated  based  on  it's
ability to  determine  (1)  if  the  bulk material  contained  1  percent or
more  of asbestos  and  (2)  what  type(s)   of  asbestos  (amosite  and/or
chrysotile) the bulk material contained.
     Two of the 50 laboratories selected for the second blind round did
not  participate  in  the round.   One  laboratory refused to  accept the
bulk  samples  because  the laboratory  manager  thought  the  RTI  surveyor
was  trying  to secure evidence  for a  pending  court case.   The  second
laboratory  was nonresponsive  (the  laboratory report for the  analysis of
the  bulk  samples was never  sent  to  the  RTI  surveyor,  after  repeated
callings over the time  period of August 1984 through November 1984).
     The qualitative  results for  the  second  blind  round  are presented
in Table 9.   Of  the  144 bulk samples  analyzed, 143 (99.3  percent)  were
classified  correctly.   A misclassification  (false positive)  was report-
ed  in one  sample (Sample C)  and   the  type  of  asbestos was  incorrectly
identified  in 29  samples (Samples  A and B).
      For Sample  A,  all  48  of the  participating  commercial  laboratories
correctly  classified the  bulk material  as  containing greater  than  1
percent asbestos, by weight.   Of  these  48  laboratories,  39 correctly
identified  both  amosite and  chrysotile in the  sample.  Eight  identifi-
cation  errors resulted because  the laboratories reported  only  one  of
the  two types of asbestos  present  in  the  sample.   This result implies
that some  laboratories  are not  conducting  a  thorough  examination of the
bulk  samples.    One   laboratory  reported   that   Sample   A  contained
anthophyllite (not  amosite  or  chrysotile),  resulting in  an additional
two  identification  errors,  for  a sample total  of 10.
      For Sample  B,  all  48 of the  participating  commercial  laboratories
correctly  classified the  bulk material  as  containing  greater  than  1
percent asbestos.   Of  these 48  laboratories,  29  correctly identified
the  type of asbestos  in the  sample as amosite and  chrysotile.  Nineteen
 identification  errors were  reported for Sample B.   These  identification
errors resulted  when only one  of  the two types of asbestos present  in
 the  sample was  reported.
                                  3-10

-------
                               TABLE 9.   QUALITATIVE RESULTS FOR THE SECOND BLIND ROUND
CO
I


Sample
ID
A


B


C





Sample
contents
Amos He, 50%
Chrysotile, 30%
Kaolinite, 20%
Amosite, 35-45%
Chrysotile, 50-60%
Carbonate, <1%
Cellulose, 15-25%
Graphite Fiber, <2%
Vermiculite, <90%
TOTAL

Number of
samples
analyzed
48


48


48


144

Number of
correct
classifications
48 (100%)


48 (100%)


47 (97.9%)


143 (99.3%)
Number of
classification errors"
False
negatives
0


0


0


0
False
positives
0


0


1


1

Number of
identification
errors0
10 (20.8%)


19 (39.6%)


0 (0%)


29 (20.1%)
            a Correctly classified  as  an  "asbestos  containing material"  as described in the Federal
              Register/Vol.  4  No.  103/Thursday,  May 27,  1982/Rules and Regulations/pg. 23370/Section
              763.103,  Definitions.

            b Samples may be misclassified  as  asbestos-containing (false positive) or as nonasbestos
              (false negative).

            c Identification errors  are  incorrect designation of the specific type of asbestos present.
              Identification and classification  errors are mutually exclusive categories; i.e., incorrect
              classifications  are  not  counted  as identification errors.

-------
     For Sample  C,  47 of the  48  participating  laboratories  correctly
classified the bulk material  as  containing less than 1  percent  asbes-
tos.   One laboratory misclassified  Sample C  as containing 5  percent
amosite.
     The distribution  of the quantitative results for the participating
laboratories in percentage of asbestos reported per sample is presented
in Table 10.   The quantitative results were not used in  determining the
laboratory performance rating.

      TABLE 10.  QUANTATITIVE RESULTS FOR THE  SECOND BLIND ROUND
Percentage of
asbestos
reported
96 - 100
86 - 95
76 - 85
66 - 75
56 - 65
46 - 55
36 - 45
26 - 35
16 - 25
6 - 15
0 - 5
TOTAL
Number of laboratories reporting

Sample A


3
9
9
8
4
12
2

1
48
Sample B

5
8
15
6
4
4
3
2
1

48
Sample C










48
48
     The distribution of  the  performance  ratings for the  second  blind
round is presented in Table  11.   Of the 48  laboratories  participating
in the second blind round, 47 achieved a performance  rating  of  3/3  (no
classification errors),  and 1 achieved a performance rating of 2/3 (One
classification error).   The laboratories scoring 3/3 recorded from zero
to  three  identification   errors.    The  laboratory  scoring  2/3  had
recorded no identification errors.
                                  3-12

-------
TABLE 11.  PERFORMANCE RATINGS FOR THE
               SECOND BLIND ROUND
Performance
rating
3/3
2/3

Number of
Classification
errors
0
1

Number of
identification errors
0123
26 14 6 1
1

Number of
laboratories
47 (97.9%)
1 (2.1%)
Total 48
                  3-13

-------
                              SECTION 4.0

                                SUMMARY

     Three aspects of  analytical  technique  are  considered  in QA Rounds
9,  10,  and  11.    First,  the  bulk  material  is  classified  as  either
asbestos-containing (greater than 1 percent) or non-asbestos-containing
(1 percent or  less).   Second,  the  specific type  of  asbestos (chryso-
tile,  amosite,  crocidolite),   nonasbestos  fibrous  material  (fibrous
glass, cellulose),  or  nonfibrous material  (calcium  carbonate, serpen-
tine)  in  the bulk material is  identified.   Third,  the  percentages of
asbestos  and  other  major  sample  constituents  are  qualified.    A
performance  rating  is   calculated  for  each  participating   laboratory
based on  the number  of bulk samples correctly classified as  containing
asbestos  (greater than 1 percent).
     The  blind round evaluates commercial laboratories on their ability
to determine (1)  if  a  bulk material  contains  greater than  1 percent of
asbestos,  and  (2) what  type  of  asbestos  the  bulk  material  contains.
The  participating  laboratories  are  randomly selected  from  the interim
listing  of  Commercial   Laboratories  with  Polarized   Light   Microscope
Capabilities  for  Bulk  Asbestos  Identification  (see  Appendix  C).   The
laboratories  participating in  the  blind round  are  not aware,  at  the
time of analysis,  that the bulk  materials  originate  from RTI under the
auspices  of  EPA's Asbestos-in-Schools Program.
     The  number  of laboratories participating  in  QA Rounds  9,  10,  and
11 were 254, 320,  and  318,  respectively.   The number of classification
errors in QA Rounds 9  ,  10, and 11  were 75, 32,  and  57,  respectively.
The  laboratories  participating  in the  program  each  received  the same
four bulk material samples to analyze per QA round.
     Fourty-eight  commercial  laboratories  participated in  Blind  Round
II,  and only one classification error resulted.   Each laboratory par-
ticipating  in  the Blind  Round  received the  same three bulk material
samples to analyze.
     Continuation of the Bulk Sample Analysis Quality Assurance Program
is  anticipated.   Any commercial  or noncommercial  laboratory that per-
forms PLM analysis of  bulk material  samples may participate.  Current-
ly,  two QA  Rounds and one Blind Round  are  planned  for each upcoming
fiscal year.
                                4-1

-------
                Appendix A



Reporting Form, Coding Form, and Instructions

-------
                        Results Reporting
                               Form
                                               BULK SAMPLE ANALYSIS
                                          QUALITY ASSURANCE PROGRAM
ro
              Laboratory I.D. #
              Sample 1.0. #
              Sample Code Assigned by Laboratory
              Analytical Method
              (enter number)
          1.  PLM
          2.  PLM with dispersion staining
          3.  PLM + X-ray diffraction
              Gross
              Sample
              Appearance
Is the sample homogeneous?
Does it contain obvious layers?
Is the sample fibrous?
                           Sample color
              Sample Treatment
              (enter number)
          1.  None
          2.  Homogenized
          3.  Other .specify
              Does the Sample Contain Any Asbestos Fibers?
              Asbestos Present (enter
              number and percent)
          1.  Amosite
          2.  Chrysotile
          3.  Crocidolite
          4.  Other, specify
              Total Percent Asbestos Present in Sample
              Other Fibrous
              Materials Present
              (enter number and
              percent)
          1.  Fibrous glass
          2.  Cellulose
          3.  Other, specify
              Nonfibrous Materials Present (description and percent)
              (Continued:  Please provide requested information on reverse side of this form.)

-------
Description of Method of Quantitation
Description of Quality Control Program (e.g., ^slides/sample, ^splits/set, use of QC samples)
Comments
Analyst  (signature required):
Affirmation:  I hereby affirm that the information appearing on this Results Reporting Form was acquired in analyses performed by the
organization submitting the results,	; that the analyses were performed by the
                                                     (name of laboratory)
person whose  signature appears above as "Analyst"; that said analyst is an employee or officer of the above-named organization; that the
instruments used in the analyses are the property of or are routinely available to said organization; and that the analyses represented by this
Results Reporting Form are typical of analytical services available to the public from said organization.
Signature                                                   Title                                 Date


Address Correction Please:	
                                                              A-3

-------
                Asbestos Bulk Sample Analysis Quality Assurance Program  Results Coding Form
                                  4-7
            9-10
Laboratory
Sample
I.D.*0
12-15




12-15




12-15


I


12



•15






I.D
#»





Round #b




Neg/Posd Asbestos Fibers Present Other Fibrous Materials Present

26
D


26
H
26

26



Typ«1* Type 2"
28-31 38-41






Percent 1f Percent 2f
33-36 43-46
I
1

1
Type 1* Type 2*
28-31 38-41






Percent 1f Percent 2f
33-36 43-46

i
1

i
i
Typ«1e Type2e
28-31 38-41






Percent 1f Percent 2f
33-36 43-46

i
1

<

Type 1* Type 28
28-31 38-41






Percent 1 Percent 2
33-36 43-46

i


(



Type 19
48-51



Percent 1f
53-56


<
Type 19
48-51



Percent 1
53-56


< i
Type 19
48-51



Percent 1f
53-56



Type 29
58-61


Percent 2
63-66

< <

Non-Fibrous
Material
Type"
68-71


Percent
73-76

i
Typeh
68-71


Percent*
73-76

<
Typeh
68-71


Percent
73-76

<
Typeh
68-71
I

Percent
73-76

i

]

,











t

'Laboratory I.D. # is first four digits on each sample.
''Round # is middle two digits.
CSample I.D. # is final four digits on each sample.
dNegative - < 1% asbestos, enter 0;
 positive • > 1% asbestos, enter 1.
'Enter type(s) of asbestos: AMOS = Amosite,
 CHRY > Chrysotile, CROC = Crocidolite, ANTH =
 Anthophyllite, TREM • Tremolite, ACTN » Actinolite,
 UNSP - unspecified.

NOTE: For materials that do not have an abbreviation, make a four letter abbreviation and explain below.
 Enter percent, note decimal placing.
9Enter other fibrous material type(s): CELL = Cellulose, FBGL =
 Fibrous glass (includes fiberglass and mineral wool), OTHR = other.

 Enter predominant non-fibrous material: CACO = Calcium carbon-
 ate, CAR8 = Carbon, CASO = Calcium sulfate (Gypsum),
 Non-fibrous glass, OTHR = other, UNSP = unspecified or unknown.
                                                       A-4

-------
                         BULK SAMPLES QUALITY  ASSURANCE  PROGRAM

Research Triangle  Institute                                     1-800-334-8571,  Ext. 5945

INSTRUCTIONS

1.  Verify that this kit contains  four  bulk material  samples.

2.  If this kit Is  Incomplete or contains  open sample packages:
       PHONE:     1-800-334-8571
       ASK FOR:   David Pasqulnl, Ext. 5945

3.  Perform a  complete analysis of  each  sample  by polarized  light microscopy,  with  or
    without dispersion staining.   X-ray diffraction  should  be  used only as  a  confirming
    technique.

4.  Results Reporting Form  (Front)

    o  Record the  results of the PLM analysis  on  the  Results Reporting Form.

    o  Record the laboratory  Identification number and  sample  identification  numbers  on
       Results Reporting Form.   The space labelled "Sample  Code Assigned  by Laboratory"
       should be  used  to record  accession numbers or other  sample  Identifiers  used  In
       laboratory  records.

       EXAMPLE:     Sample Labels:  2750-10-3728
                                    2750-10-1494
                                    2750-10-9673
                                    2750-10-7307
       Laboratory  ID #2750


           Sample  ID*     10-3728      10-1494      10-9673      10-7307


    o  Fill In all  blocks for each  analysis performed,  using zeros  or "none" where neces-
       sary.   In  categories offering  numbered choices, write  the  correct number In the
       appropriate  block, followed by  a percent  value or  comment.   Reporting  forms with
       Incomplete Information will  not  be  evaluated.

    o  Answer the  question:  "Does  the  sample  contain any  asbestos  fibers?",  either "yes"
       or "no".   Answer "yes" If any asbestos  fibers  are seen  and  "no"  If  none are seen.
       The  answer "yes"  Is not  a statement that the sample   Is an  "asbestos-containing
       material"  (see below).

    o  Under "Asbestos Present", report  the amount  of each type of  asbestos  present as a
       percentage  of  the total  material  In the  sample.   Do  not   report  the  amount  of
       asbestos as  a percentage of fibrous components only.    If no asbestos  Is present,
       report "None" or  "Of".   If asbestos Is present and  the amount  Is  less  than  or
       equal to 1  percent, report  "trace", "<1<", or  "_
-------
5.  Results Reporting Form (Reverse)

    o  Complete the reverse side of the Results Reporting Form.

    o  Provide descriptions of  the procedures used for quantitative  analysis and of  the
       routine quality control measures used  for  bulk sample analysis.   Information  pro-
       vided  In  previous  rounds need  not  be  repeated  If still  applicable.   Additional
       Information regarding sample preparation and analytical  procedures  may be supplied
       In the space provided for comments.

    o  The analyst's  signature  Is  required.    Reporting  forms submitted without  required
       signatures will not be evaluated.

    o  The affirmation states that the results being reported  were obtained  In  analyses
       performed by the laboratory submitting  those results.  Complete the statement  with
       the name of the laboratory  as  It appears  In  the  cover letter address.   The signa-
       ture of the laboratory manager or other company officials  responsible for analyti-
       cal services (the analyst,  If  applicable)  Is required.  Reporting  forms  submitted
       without required signatures will not be evaluated.

    o  Please provide changes or corrections  In  the laboratory mailing address  If appli-
       cable.

6.  Results Coding Form

    Transfer the data  from the Results Reporting  Form to the  Results Coding Form  using
    the codes provided at the bottom of the form.   Notice that the percentages  are  to be
    recorded underneath the material type  in the first  four  columns.    Fill  in  only  those
    blocks that apply, and leave the others blank.  Please print  legibly  because the data
    on the  Results Coding Form Is the  data  on  which  your  performance  rating  will  be
    based.

7.  Layered Samples

    Often samples of  Insulation materials  will contain more  than one "layer" or  type of
    material.  When It Is apparent that a  sample contains more  than one layer,  each  layer
    should be  analyzed  separately. For  the  purposes of  this  program,  assume  that  each
    layer comprises  an  equal  volume  of  the  sample,  and  report only  one  value  for  each
    sample  regardless of  the  number  of  layers  that are present.   For   example:    If  a
    sample Is made up of two different layers, and one  layer  Is 60? amoslte and  the  other
    layer  Is 40%  chrysotlle,  the  correct reporting  values would be 30$ amoslte,  20$
    chrysotile, and 50% total asbestos.

8.  Retain all  samples  for future  reference  following receipt of  the round  results and
    statistical summary.

9.  Return the Results Reporting Form and Results Coding Form by  the date  indicated in
    the cover  letter.  Mall to:

             David A. Pasquinl, C.I.H.
             Research Triangle  Institute
             BuIIdIng 6
             Post Office Box  12194
             Research Triangle Park, North Carolina   27709-2194

                  LATE RETURNS WILL NOT BE EVALUATED
                                          A-6

-------
        Appendix B



Sample Report to Laboratories

-------
                                                                   ASBESTOS BULK  SAMPLE  ANALYSIS Q.A.  PROGRAM
                                                                               RESULTS OF  ROUND 11
                                                                               JANUARY  11,  1985
                       Mr.  Gene Yonkin
                       Chemical & Geological Labs of Alaska
                       5633 B Street
                       Anchorage, AK  99502
                                                                   Laboratory
                                                                   I.D.  Number
                                                                   0102
    False  Negatives:    0
    Flase  Positives:    1
    Performance  Rating:    3/4
Lot &
Sample
I.D.
Number
A)
2812
B)
1023
C)
0431
F_POS
D)
5743
                   Results from
                   Laboratory Number 0102
                     Asbestos (%)

                     Other Fibrous Material  (%)

                     Nonfibrous Material  (%)
                                                100.0 OTI1R
                                                                           90.0 CROC
                                                                                              10.0 NF
                                                                                                     10.0 ACTN
                                                                                                                        90.0  NF
                                                                                                                               100.0 FBGL
CO

ro
Qualitative Results from
Reference Laboratory
  Asbestos

  Other Fibrous Material

  Nonfibrous Material
NONE
OTHR
NONE
CROC
NONE
OTHR
NONE
OTHR
CACO
NONE
CARB
NONE
                   Summary of Quantitative  Results
                     Percent  Asbestos-Percentiles
                        50% - Median  (N=2?4)                           0 0

                       100% - Maximum                                90 0
                        95%                                           0.0
                        75%                                           0 0
                        25%                                           0 0
                         5%                                           0.0
                         0% - Minimum                                 0.0

                     Percent  Other  Fibrous  Material
                       OFM -  Median (N)                            100.0(261)

                     Percent  Nonfibrous Material
                       NF  - Median  (N)

                   Asbestos Abbreviations
                     ACTN=Actinolite              CROC=CROCIOOLITE
                   Other Fibrous Material Abbreviations
                     FBGL=Fibrous Glass           CARB= Carbon           OTHR=Other
                   Nonfibrous Material Abbreviations
                     CACO=Calcium Carbonate
                                                                             85.0

                                                                            100.0
                                                                            100.0
                                                                             95.0
                                                                             70.0
                                                                             30.0
                                                                             0.0
                                                                           15.0(222)
   0.0

  90.0
  20.0
   0.0
   0.0
   0.0
   0.0
10 0(118)


90.0(253)
 0.0

99.0
 0.0
 0.0
 0.0
 0.0
 0.0
                                                                                                                               100.0(264)

-------
      Appendix C



Interim Listing Number 18

-------
    Commercial Laboratories with  Polarized
        Light  Microscope Capabilities for
            Bulk Asbestos  Identification
                         Interim Listing
                           Number 18
                   EPA Bulk Analysis Round 11
                           Prepared by:
                      Research Triangle Institute
                          P.O. Box 12194
                   Research Triangle Park, NC 27709
                           Prepared for

Environmental Monitoring Systems Laboratory       Office of Toxic Substances
U.S. Environmental Protection Agency            U.S. Environmental Protection Agency
Research Triangle Park, NC 27711              Washington, DC 20460
                           March 1985
                              C-2

-------
                               INTRODUCTION

     The following laboratories participated in the current round of the
U.S.  Environmental Protection Agency's (EPA) bulk asbestos sample quality
assurance program.  Laboratories are listed with their performance scores
for this and previous rounds in which they participated.   Laboratory per-
formance was assessed on the basis of correct identification of "positive"
(containing >1 percent asbestos) and "negative" (containing <1 percent
asbestos) samples.  Reductions of correct scores (3/3, 4/4, or 8/8) were,
made only for the reporting of false positives (nonasbestos sample reported
as containing >1 percent asbestos) or false negatives (1 percent or less
asbestos reported in an asbestos-containing sample), and not for the mis-
identification of individual asbestos mineral species.  Although the cri-
terion is lenient, it recognizes the basic concern of the public—the
presence or absence of asbestos fibers in a submitted sample.   Four separate
bulk samples were sent to each laboratory in Rounds 1, 2, 4, 5, 6, 7, 8,
10, and 11; eight were sent in Round 3.   Three samples were evaluated in
Round 9.  All analyses were performed by polarized light microscopic (PLM)
analysis.  Where numerical  evaluations are omitted, an alphabetical character
is included to reference the description below.
          Letter                            Description
             D                The laboratory was disqualified in that
                              round.
             N                The laboratory received samples but did
                              not participate in the round.
             P                The laboratory participated as a noncom-
                              mercial laboratory; performance scores
                              therefore are not reported.
             U                The laboratory did not receive samples
                              in that round.
                                     C-3

-------
     The quality assurance program is not designed for laboratory accredi-
tation and does not certify or endorse participating laboratories.   This
list of program participants is provided as a source of analytical  labora-
tories by the EPA Asbestos-in-Schools Program.   Updated lists  of partic-
ipating laboratories and further information on the quality assurance
program, sampling and analysis of asbestos-containing materials, and the  EPA
Asbestos-in-Schools Program is available from the Asbestos Technical Infor-
mation Service at (800)334-8571 (Extension 6741).
                          Regional Organizations
                                     C-4

-------
                                   REGION 1
Mr. Jim Kenny
Aetna Insurance Company
Environmental Health Laboratory
94 Murphy Road
Hartford, CT  06114
203/522-3814
Mr. Harold C. Kraus
Environmental Technology
P. 0. Box 127
West Hartford, CT  06107
203/521-6820
Mr. Edward B. Engel
Aetna Life & Casualty, Engineering Div.
Environmental Health Unit
151 Farmington Avenue
Hartford, CT  06156
203/273-3445
Mr. Wiech
Environmental Associates, Inc.
P. 0. Box 224
Fairfield, CT  06430
203/259-6142
Ronald E. McCullen
Travelers Insurance-Engr Lab
248 Continental Plaza
Hartford, CT  06115
203/277-7533
Sally E. Reffner
TAKA
97 Ocean Drive East
Stamford, CT  06902
203/356-8977
Stephan W. Campbell-ESU L
Hartford Insurance Group
Hartford Plaza
Hartford, CT  06115
203/547-4557
RND 1:
RND 4:
RND 7:
RND10:
RND 1:
RND 4:
RND 7:
RND10:
RND 1:
RND 4:
RND 7:
RND10:
RND 1:
RND 4:
RND 7:
RND10:
RND 1:
RND 4:
RND 7:
RND10:
RND 1:
RND 4:
RND 7:
RND10:
RND 1:
RND 4:
RND 7:
RND10:
U
4/4
3/4
4/4
U
N
4/4
4/4
U
4/4
2/4
4/4
U
3/4
4/4
4/4
U
U
4/4
4/4
U
U
4/4
4/4
U
U
4/4
4/4
RND 2:
RND 5:
RND 8:
RND11:
RND 2:
RND 5:
RND 8:
RND11:
RND 2:
RND 5:
RND 8:
RND11:
RND 2:
RND 5:
RND 8:
RND11:
RND 2:
RND 5:
RND 8:
RND11:
RND 2:
RND 5:
RND 8:
RND11:
RND 2:
RND 5:
RND 8:
RND11:
U
4/4
4/4
4/4
4/4
4/4
4/4
4/4
U
4/4
4/4
4/4
U
4/4
4/4
3/4
U
U
4/4
4/4
U
U
4/4
4/4
U
U
4/4
4/4
RND
RND
RND

RND
RND
RND

RND
RND
RND

RND
RND
RND

RND
RND
RND

RND
RND
RND

RND
RND
RND

3:
6:
9:

3:
6:
9:

3:
6:
9:

3:
6:
9:

3:
6:
9:

3:
6:
9:

3:
6:
9:

U
4/4
3/3

D
4/4
3/3

6/8
4/4
3/3

U
4/4
3/3

U
U
3/3

U
4/4
3/3

U
U
3/3

                                   C-5

-------
                                   REGION  1
Thomas F. Hatch
Peck Laboratories, Inc.
P. 0. Box 947
Kennebunk, ME  04043
207/985-6116
Ms. Mary Kozik
GCA Technology Division
213 Burlington Road
Bedford, MA  01730
617/275-5444
Cathy L. Oakes
K-Chem Laboratories
46 Clayton Street
Boston, MA  02122
617/436-7181
Ralph Berger
Skinner & Sherman Lab
300 2nd Avenue, Box 521
Waltham, Ma  02254
617/890-7200
Mr. Robert L. MacDonald
Eastern Analytical Laboratories, Inc.
149 Rangeway Road
Bill erica, MA  01862
617/272-5212
James E.  Dennison
Dennison Environmental
P. 0. Box 2526
Woburn, MA  01888
617/938-8508
Glen Sylvester                             _ _. _
Certified Engineering & Testing Co. Inc. RND 4: U
166 Schoosett Street
Pembroke, MA  02359
617/826-7336
RND 1:
RND 4:
RND 7:
RND10:
RND 1:
RND 4:
RND 7:
RND10:
RND 1:
RND 4:
RND 7:
RND10:
RND 1:
RND 4:
RND 7:
RND10:
RND 1:
RND 4:
RND 7:
RND10:
RND 1:
RND 4:
RND 7:
RND10:
RND 1:
RND 4:
RND 7:
RND10:
U
U
U
3/4
4/4
4/4
4/4
4/4
U
U
N
4/4
U
U
3/4
4/4
4/4
4/4
4/4
4/4
U
U
U
U
U
U
U
4/4
RND 2:
RND 5:
RND 8:
RND11:
RND 2:
RND 5:
RND 8:
RND11:
RND 2:
RND 5:
RND 8:
RND11:
RND 2:
RND 5:
RND 8:
RND11:
RND 2:
RND 5:
RND 8:
RND11:
RND 2:
RND 5:
RND 8:
RND11:
RND 2:
RND 5:
RND 8:
RND11:
U
U
U
3/4
N
4/4
4/4
4/4
U
U
4/4
4/4
U
U
4/4
4/4
4/4
4/4
4/4
4/4
U
U
U
4/4
U
U
4/4
3/4
RND
RND
RND

RND
RND
RND

RND
RND
RND

RND
RND
RND

RND
RND
RND

RND
RND
RND

RND
RND
RND

3:
6:
9:

3:
6:
9:

3:
6:
9:

3:
6:
9:

3:
6:
9:

3:
6:
9:

3:
6:
9:

U
U
N

8/8
4/4
3/3

U
U
3/3

U
4/4
3/3

8/8
4/4
3/3

U
U
U

U
U
3/3

                                   C-6

-------
                                   REGION 1
Fred Boyle
Hub Testing Laboratory
95 Beaver Street
Waltham, MA  02154
617/893-8330
Mr. James Litrides
Briggs Associates Inc.
400 Hingham Street
Rock!and, MA  02370
617/871-6040
Thomas E. Veratti
CON-TEST, Inc.
105 Hillside Drive
East Longmeadow, MA  01028
413/525-1198
Dr. Spooner
Hygeia, Inc.
1380 B Main Street
Waltham, MA  02154
617/647-9475
Samual J. Covino
ESA
43 Wiggins Avenue
Bedford, MA  01730
617/275-0100
Dr. Fred E. Tibbetts
Tibbetts Engineering Corporation
210 Deane Street
New Bedford, MA  02746
617/996-5633
Dr. Robert J. Emerson
Shelburne Laboratories, Inc.
P. 0.  Box 458
Shelburne, VT  05482
802/425-3438
RND 1:
RND 4:
RND 7:
RND10:
RND 1:
RND 4:
RND 7:
RND10:
RND 1:
RND 4:
RND 7:
RND10:
RND 1:
RND 4:
RND 7:
RND10:
RND 1:
RND 4:
RND 7:
RND10:
RND 1:
RND 4:
RND 7:
RND10:
RND 1:
RND 4:
RND 7:
RND10:
U
3/4
3/4
N
U
4/4
4/4
4/4
U
U
U
4/4
U
U
U
4/4
U
U
3/4
4/4
U
4/4
4/4
3/4
U
U
U
4/4
RND 2:
RND 5:
RND 8:
RND11:
RND 2:
RND 5:
RND 8:
RND11:
RND 2:
RND 5:
RND 8:
RND11:
RND 2:
RND 5:
RND 8:
RND11:
RND 2:
RND 5:
RND 8:
RND11:
RND 2:
RND 5:
RND 8:
RND11:
RND 2:
RND 5:
RND 8:
RND11:
U
4/4
4/4
4/4
3/4
4/4
4/4
3/4
U
U
U
4/4
U
U
4/4
3/4
U
U
4/4
4/4
U
4/4
4/4
4/4
U
U
U
4/4
RND
RND
RND

RND
RND
RND

RND
RND
RND

RND
RND
RNO

RND
RND
RND

RND
RND
RND

RNO
RND
RND

3:
6:
9:

3:
6:
9:

3:
6:
9:

3:
6:
9:

3:
6:
9:

3:
6:
9:

3:
6:
9:

U
N
2/3

8/8
4/4
3/3

U
U
3/3

U
U
3/3

U
4/4
3/3

8/8
4/4
3/3

U
U
3/3

                                   C-7

-------
                                   REGION 2
Mr.  Joseph E. Wilson
Environmental Health Protection
Consultants, Inc.
46 Ivy Lane
Cherry Hill, NJ  08002
609/779-1372
Gordon K. Yetter
Alternative Ways, Inc.
RD 2 - Box 205
Colony Place
Swedesboro, NJ  08085
609/871-5538
J. Sheraard
S-R Analytical, Inc.
28 Springdale  Road
P.O. Box 4201
Cherry Hill, NJ  08003
609/541-6700
James F. McVeigh
Atlantic Environmental Inc.
112 Main Road
Montville, NJ  07045
201/335-5756
Douglas Campbell
PSE & G Research Corporation
200 Boyden Avenue
Maplewood, NJ  07040
201/761-1390
Kirit H. Vora
Clayton Environmental Consultants,  Inc.
160  Fieldcrest Avenue
Raritan Center
Edison, NJ  08837
201/225-6040
John  E.  Stillman
Exxon Corp.
Industrial  Hyg. Analytical  Service  Lab.
P.  0.  Box  235,  Mettlers  Rd.
East  Millstone, NJ   08873
RND 1:
RND 4:
RND 7:
RND10:
RND 1:
RND 4:
RND 7:
RND10:
RND 1:
RND 4:
RND 7:
RND10:
RND 1:
RND 4:
RND 7:
RND10:
RND 1:
RND 4:
RND 7:
RND10:
RND 1:
RND 4:
RND 7:
RND10:
RND 1:
RND 4:
RND 7:
RND10:
U
4/4
3/4
4/4
U
U
2/4
4/4
U
U
U
4/4
U
U
3/4
3/4
U
U
U
4/4
4/4
4/4
4/4
4/4
U
U
U
4/4
RND 2:
RND 5:
RND 8:
RND11:
RND 2:
RND 5:
RND 8:
RND11:
RND 2:
RND 5:
RND 8:
RND11:
RND 2:
RND 5:
RND 8:
RND11:
RND 2:
RND 5:
RND 8:
RND11:
RND 2:
RND 5:
RND 8:
RND11:
RND 2:
RND 5:
RND 8:
RND11:
U
4/4
4/4
3/4
U
U
4/4
4/4
U
U
U
4/4
U
U
4/4
3/4
U
U
U
3/4
3/4
4/4
4/4
3/4
U
U
U
4/4
RND
RND
RND

RND
RND
RND

RND
RND
RND

RND
RND
RND

RND
RND
RND

RND
RND
RND

RND
RND
RND

3:
6:
9:

3:
6:
9:

3:
6:
9:

3:
6:
9:

3:
6:
9:

3:
6:
9:

3:
6:
9:

8/8
4/4
3/3

U
N
3/3

U
U
N

U
U
3/3

U
U
U

8/8
4/4
3/3

U
U
3/3

                                   C-8

-------
                                   REGION 2
Ms. Jane Clarke-James
Testwell-Craig Testing Laboratories
565 East Harding Highway
Mays Landing, NJ  08330
609/625-1700
J. Stephen Duerr
Structure Probe, Inc.
230 Forrest Street
Metuchen, NJ  08840
201/549-9350
Dr. Sor
Shimel and Sor Testing Laboratories
P. 0.  Box 78
East Hanover, NJ  07936
201/887-8808
James J. Weitzman
Kaselaan & D'Angelo Associates, Inc.
215 White Horse Pike
Haddon Heights, NJ  08035
609/227-7841
Mr. W. B. Rossnagle
Rossnagle and Associates, Inc.
234 Route 70
Medford, NJ  08055
609/654-1441
David Kichula
Princeton Testing Laboratory
P.  0. Box 3108
Princeton, NJ  08540
609/452-9050
Gary Hahn
Ecology & Environmental, Inc.
P.  0.  Box D, 195 Sugg Road
Buffalo, NY  14225
716/631-0360
RND 1:
RND 4:
RND 7:
RND10:
RND 1:
RND 4:
RND 7:
RND10:
RND 1:
RND 4:
RND 7:
RND10:
RND 1:
RND 4:
RND 7:
RND10:
RND 1:
RND 4:
RND 7:
RND10:
RND 1:
RND 4:
RND 7:
RND10:
RND 1:
RND 4:
RND 7:
RND10:
N
4/4
4/4
4/4
U
U
U
4/4
U
U
U
4/4
U
U
4/4
4/4
N
N
I
I
3/4
N
I
4/4
U
U
3/4
4/4
RND 2:
RND 5:
RND 8:
RND11:
RND 2:
RND 5:
RND 8:
RND11:
RND 2:
RND 5:
RND 8:
RND11:
RND 2:
RND 5:
RND 8:
RND11:
RND 2:
RND 5:
RND 8:
RND11:
RND 2:
RND 5:
RND 8:
RND11:
RND 2:
RND 5:
RND 8:
RND11:
4/4
4/4
4/4
3/4
U
U
4/4
3/4
U
U
3/4
4/4
U
4/4
4/4
4/4
N
N
I
3/4
3/4
I
4/4
4/4
U
U
4/4
2/4
RND
RND
RND

RNO
RND
RND

RND
RND
RND

RND
RND
RND

RND
RND
RND

RND
RND
RND

RND
RND
RND

3:
6:
9:

3:
6:
9:

3:
6:
9:

3:
6:
9:

3:
6:
9:

3:
6:
9:

3:
6:
9:

7/8
N
N

U
U
3/3

U
U
2/3

U
4/4
3/3

D
I
I

8/8
I
3/3

U
4/4
3/3

                                   C-9

-------
                                   REGION 2
Mr. Thomas A. Kubic
TAKA Asbestos Analytical Services
P. 0. Box 208
Greenlawn, NY  11740
516/261-2117
Dr. Malcolm Newman
Inter-City Testing & Consulting Corp.
159 Great Neck Road
Great Neck, NY  11021
516/829-8762
Doug Friend
Friend Laboratory, Inc.
446 Braod Street
Waverly, NY 14892 1445
607/565-2893
Ronald Bielinski
Adelaide Envr Health Associates
142 Riverside Drive
Binghamton, NY  13905
607/722-6839
Ved P.  Kukreja
Enviro-Probe, Inc.
1424 Williamsbridge Road
Bronx,  NY  10461
212/863-0045
Eva Gal son
Gal son Technical Services
6601 Krikville Road
East Syracuse, NY  13057
315/437-7181
Dr.  Jesse H.  Bidanset
J.  H.  Bidanset & Associates
167 Willis Avenue
Mineola, NY  11501
516/747-8400
RND 1:
RND 4:
RND 7:
RND10:
RND 1:
RND 4:
RND 7:
RND10:
RND 1:
RND 4:
RND 7:
RND10:
RND 1:
RND 4:
RND 7:
RND10:
RND 1:
RND 4:
RND 7:
RND10:
RND 1:
RND 4:
RND 7:
RND10:
RND 1:
RND 4:
RND 7:
RND10:
4/4
4/4
4/4
4/4
4/4
4/4
4/4
4/4
U
U
2/4
3/4
U
U
U
4/4
U
U
N
4/4
U
4/4
4/4
4/4
4/4
4/4
4/4
4/4
RND 2:
RND 5:
RND 8:
RND11:
RND 2:
RND 5:
RND 8:
RND11:
RND 2:
RND 5:
RND 8:
RND11:
RND 2:
RND 5:
RND 8:
RND11:
RND 2:
RND 5:
RND 8:
RND11:
RND 2:
RND 5:
RND 8:
RND11:
RND 2:
RND 5:
RND 8:
RN011:
4/4
4/4
4/4
4/4
4/4
4/4
4/4
4/4
U
U
3/4
4/4
U
U
U
4/4
U
U
4/4
4/4
U
4/4
4/4
4/4
4/4
4/4
4/4
4/4
RND
RND
RND

RND
RND
RND

RND
RND
RND

RND
RND
RND

RND
RND
RND

RND
RND
RND

RND
RND
RND

3:
6:
9:

3:
6:
9:

3:
6:
9:

3:
6:
9:

3:
6:
9:

3:
6:
9:

3:
6:
9:

8/8
4/4
3/3

8/8
4/4
3/3

U
U
2/3

U
U
U

U
U
3/3

U
4/4
3/3

8/8
4/4
3/3

                                  C-10

-------
                                    REGION  2
Mr. John Gaspari
New York Testing Laboratory
81 Urban Avenue
Westbury, NY  11590
516/334-7770
RND 1: U
RND 4: 4/4
RND 7: 4/4
RND10: 4/4
RND 2:
RND 5:
RND 8:
RND11:
U
4/4
4/4
4/4
RND 3: 8/8
RND 6: 4/4
RND 9: 3/3
Susan Marie Viet
KEMRON
755 New York Avenue
Huntington, NY  11743
516/427-0950
RND 1:  4/4
RND 4:  4/4
RND 7:  3/4
RND10:  4/4
RND 2:
RND 5:
RND 8:
RND11:
4/4
4/4
4/4
4/4
RND 3: 8/8
RND 6: 4/4
RND 9: 3/3
                                   C-ll

-------
                                    REGION  3
Naresh C. Batta
Batta Environmental Associates
P. 0. Box 9722
Newark, DE  19714 9722
302/737-3376
Raymond C. Crippen, Ph.D.
Crippen Laboratories, Inc.
4027 New Castle Avenue
New Castle, DE  19720
302/571-8882
Gary A. Hayes
V. J. Schuler Associates, Inc.
P. 0. Box 138
Middletown, DE  19709
302/378-9881
Mr. Frank Fitzpatrick
Biospherics, Inc.
4928 Wyaconda Road
Rockville, MD  20852
301/770-7700
Camille J. Carraway
Oneil M. Banks Inc.
125 N.  Main Street
Bel Air, MD  21614
301/879-4676
Michael Cirri
Aerosol Monitoring and Analysis,
246 Cockeysville Road
P.  0.  Box 687
Hunt Valley, MD  21030
301/666-5105
Marc Hal pern
Tracer Jitco, Inc.
1601 Research Blvd.
Rockville, MD  20850
301/984-2800
Inc.
RND 1:
RND 4:
RND 7:
RND10:
RND 1:
RND 4:
RND 7:
RND10:
RND 1:
RND 4:
RND 7:
RND10:
RND 1:
RND 4:
RND 7:
RND10:
RND 1:
RND 4:
RND 7:
RND10:
RND 1:
RND 4:
RND 7:
RND10:
RND 1:
RND 4:
RND 7:
RND10:
U
U
U
4/4
U
U
N
4/4
U
U
U
U
U
4/4
4/4
4/4
U
U
U
4/4
U
U
4/4
4/4
U
U
U
4/4
RND 2:
RND 5:
RND 8:
RND11:
RND 2:
RND 5:
RND 8:
RND11:
RND 2:
RND 5:
RND 8:
RND11:
RND 2:
RND 5:
RND 8:
RND11:
RND 2:
RND 5:
RND 8:
RND11:
RND 2:
RND 5:
RND 8:
RND11:
RND 2:
RND 5:
RND 8:
RND11:
U
U
U
4/4
U
U
3/4
3/4
U
U
U
4/4
4/4
4/4
4/4
3/4
U
U
U
3/4
U
U
4/4
3/4
U
U
4/4
4/4
RND
RND
RND

RND
RND
RND

RND
RND
RND

RND
RND
RND

RND
RND
RND

RND
RND
RND

RND
RND
RND

3:
6:
9:

3:
6:
9:

3:
6:
9:

3:
6:
9:

3:
6:
9:

3:
6:
9:

3:
6:
9:

U
U
U

U
U
2/3

U
U
U

8/8
4/4
3/3

U
U
3/3

U
U
3/3

U
U
N

                                   C-12

-------
                                   REGION 3
Mr.  Mark R.  Banister
Microbac, Inc.
Erie Testing Laboratory Division
2401 W. 26th St.
Erie, PA  16506
814/833-4790
John M. Lang
Universial Laboratories
P. 0. Box 58040
Pittsburgh, PA  15209
412/821-5411
Mr. G. E. Williams
Pittsburgh Testing Laboratory
850 Poplar Street
Pittsburgh, PA  15220
412/922-4000
Frank J. Kernozek
Betz Converse Murdoch  Laboratory
521 W. Germantown Pike
Norristown, PA  19401
215/825-0447
Richard  L. Mason
FREE-COL Division
Freeport Brick Company
P. 0. Box 557, Cotton Road
Meadville, PA  16335
814/724-6242
Mr.  Spensor Watts
Spotts,  Stevens, &  McCoy
345  N. Wyomissing Blvd.
Wyomissing, PA  19610
215/376-6581
 Barbara  J.  Felty
 Lancaster  Laboratories  Inc.
 2425  New Holland  Pike
 Lancaster,  PA   17601
 717/656-2301
RND 1:
RND 4:
RND 7:
RND10:
RND 1:
RND 4:
RND 7:
RND10:
RND 1:
RND 4:
RND 7:
RND10:
RND 1:
RND 4:
RND 7:
RND10:
RND 1:
RND 4:
RND 7:
RND10:
RND 1:
RND 4:
RND 7:
RND10:
RND 1:
RND 4:
RND 7:
RND10:
4/4
4/4
4/4
4/4
U
U
U
4/4
-U
4/4
4/4
4/4
U
U
3/4
4/4
U
U
U
4/4"
U
I
I
4/4
U
U
4/4
4/4
RND 2:
RND 5:
RND 8:
RND11:
RND 2:
RND 5:
RND 8:
RND11:
RND 2:
RND 5:
RND 8:
RND11:
RND 2:
RND 5:
RND 8:
RND11:
RND 2:
RND 5:
RND 8:
RND11:
RND 2:
RND 5:
RND 8:
RND11:
RND 2:
RND 5:
RND 8:
RND11:
3/4
4/4
4/4
4/4
U
U
U
3/4
D
4/4
4/4
4/4
U
U
4/4
4/4
U
U
4/4
4/4
U
I
I
3/4
U
4/4
4/4
4/4
RND
RND
RND

RND
RND
RND

RND
RND
RND

RND
RND
RND

RND
RND
RND

RND
RND
RND

RND
RND
RND

3:
6:
9:

3:
6:
9:

3:
6:
9:

3:
6:
9:

3:
6:
9:

3:
6:
9:

3:
6:
9:

8/8
4/4
3/3

U
U
U

8/8
4/4
3/3

U
U
3/3

U
U
3/3

N
I
I

U
4/4
3/3

                                  C-13

-------
                                   REGION 3
Dr.  Roy S.  Anderson
Comprehensive Chemical Consulting
514 Concord Or.
Broomal1,  PA  19008
215/353-3015
Marianne C. Kaschak
Industrial Health Foundation, Inc.
34 Penn Circle West
Pittsburgh, PA  15206
412/363-6600
Nancy Kotsko
Air Quality Services
4527 Clairton Boulevard
Pittsburgh, PA  15236
Ellie Chapman
Industrial Hygiene & Occup. Med Lab
A Division of American Medical Lab,
11091 Main Street
Fairfax, VA  22030
703/691-9100
W. Corey Thompson
Versar Inc.
6850 Versar Center
Springfield, VA  22151
703/750-3000
Edwin Cox, III
Commonwealth Laboratory, Inc.
Chemists Building
2209 East Broad Street
Richmond, VA  23223
804/648-8358
Kent Schoemaker
Industrial Hygiene Laboratory
Newport News Shipbuilding
4101 Washington Avenue
Newport News, VA  23607
804/380-2000
Inc.
RND 1:
RND 4:
RND 7:
RND10:
RND 1:
RND 4:
RND 7:
RND10:
RND 1:
RND 4:
RND 7:
RND10:
RND 1:
RND 4:
RND 7:
RND10:
RND 1:
RND 4:
RND 7:
RND10:
RND 1:
RND 4:
RND 7:
RND10:
RND 1:
RND 4:
RND 7:
RND10:
U
U
U
4/4
U
U
U
4/4
U
N
4/4
4/4
U
4/4
4/4
4/4
U
U
4/4
4/4
U
U
4/4
4/4
U
U
4/4
4/4
RND 2:
RND 5:
RND 8:
RND11:
RND 2:
RND 5:
RND 8:
RND11:
RND 2:
RND 5:
RND 8:
RND11:
RND 2:
RND 5:
RND 8:
RND11:
RND 2:
RND 5:
RND 8:
RND11:
RND 2:
RND 5:
RND 8:
RND11:
RND 2:
RND 5:
RND 8:
RND11:
U
U
U
3/4
U
U
4/4
3/4
U
4/4
3/4
4/4
U
4/4
4/4
4/4
U
U
4/4
4/4
U
U
4/4
4/4
U
4/4
4/4
4/4
RNO
RND
RND

RND
RND
RND

RND
RND
RND

RND
RND
RND

RND
RND
RNO

RND
RND
RND

RND
RND
RND

3:
6:
9:

3:
6:
9:

3:
6:
9:

3:
6:
9:

3:
6:
9:

3:
6:
9:

3:
6:
9:

U
U
3/3

U
U
3/3

U
4/4
3/3

U
4/4
3/3

U
U
3/3

U
U
3/3

U
4/4
3/3

                                   C-14

-------
                                   REGION 3
Dr. Joseph H. Guth
Interscience Research
2614 Wyoming Avenue
Norfolk, VA  23513
804/853-8813
Mr. James Calpin
Analytics
P.O. Box 25249
Richmond, VA  23260
804/353-8973
Steven R. Pond
Environmental Laboratories, Inc.
103 S. Leadbetter Road
Ashland, VA  23005
804/798-1589
Mr. Robert Walker
Marine Chemist Service, Inc.
P. 0.  Box 6257
Newport News, VA  23606
804/877-9933
John Connover
263 Simpkins Ct.
Mechanicsville, VA  23111
804/746-7820
RND 1:
RND 4:
RND 7:
RND10:
RND 1:
RND 4:
RND 7:
RND10:
RND 1:
RND 4:
RND 7:
RND10:
RND 1:
RND 4:
RND 7:
RND10:
RND 1:
RND 4:
RND 7:
RND10:
4/4
4/4
4/4
4/4
U
4/4
4/4
4/4
U
U
4/4
4/4
U
4/4
4/4
4/4
U
U
4/4
4/4
RND 2:
RND 5:
RND 8:
RND11:
RND 2:
RND 5:
RND 8:
RND11:
RND 2:
RND 5:
RND 8:
RND11:
RND 2:
RND 5:
RND 8:
RND11:
RND 2:
RND 5:
RND 8:
RND11:
3/4
4/4
4/4
4/4
U
4/4
4/4
4/4
U
4/4
4/4
4/4
U
4/4
4/4
3/4
U
4/4
4/4
4/4
RND
RND
RND

RND
RND
RND

RND
RND
RND

RND
RND
RND

RND
RND
RND

3:
6:
9:

3:
6:
9:

3:
6:
^

3:
6:
9:

3:
6:
9:

8/8
4/4
3/3

8/8
4/4
3/3

U
4/4
3/3

8/8
4/4
3/3

U
4/4
N

                                    C-15

-------
                                   REGION 4
Dr.  Charles Ray, Jr.
Safety and Environmental Affairs
300 Nuclear Science Bldg.
Auburn University
Auburn, AL  36849
205/826-4870
Mr.  M.  A. Beg
American Microscopy Laboratory
29 Heritage Hills
Tuscaloosa, AL  35406
205/345-2555
Jack E. Davis
Tuscaloosa Testing Laboratory, Inc.
3516 Greensboro Avenue
P. 0. Box 1094
Tuscaloosa, AL  35403
205/345-0816
James C. Sciple
Thompson Engineering Testing
3707 Cottage Hill Road
P. 0. Drawer 9637
Mobile, AL  36609
205/666-2443
Randy Ogle
Safe State Program
University of Alabama
P. 0. Box 6005
Tuscaloosa, AL  35486
205/348-7136
H. Kenneth Dillon
Southern Research Institute
2000 Ninth Avenue South
P. 0. Box 55305
Birmingham, AL  35255-5305
205/323-6592
Steven E. Jones
Applied Technology Consultants
1800-B Airport Road
Opelika, AL  36801
205/749-6366
RND 1:
RND 4:
RND 7:
RND10:
RND 1:
RND 4:
RND 7:
RND10:
RND 1:
RND 4:
RND 7:
RND10:
RND 1:
RND 4:
RND 7:
RND10:
RND 1:
RND 4:
RND 7:
RND10:
RND 1:
RND 4:
RND 7:
RND10:
RND 1:
RND 4:
RND 7:
RND10:
U
U
4/4
4/4
4/4
4/4
4/4
4/4
U
U
4/4
4/4
U
U
4/4
4/4
U
4/4
4/4
4/4
U
U
U
4/4
U
U
U
4/4
RND 2:
RND 5:
RND 8:
RND11:
RND 2:
RND 5:
RND 8:
RND11:
RND 2:
RND 5:
RND 8:
RND11:
RND 2:
RND 5:
RND 8:
RND11:
RND 2:
RND 5:
RND 8:
RND11:
RND 2:
RND 5:
RND 8:
RND11:
RND 2:
RND 5:
RND 8:
RND11:
U
U
4/4
4/4
3/4
4/4
4/4
4/4
U
U
4/4
4/4
U
U
4/4
4/4
U
4/4
4/4
4/4
U
U
4/4
4/4
U
U
4/4
4/4
RND
RND
RND

RND
RND
RND

RND
RND
RND

RND
RND
RND

RND
RND
RND

RND
RND
RND

RND
RND
RND

3:
6:
9:

3:
6:
9:

3:
6:
9:

3:
6:
9:

3:
6:
9:

3:
6:
9:

3:
6:
9:

U
4/4
3/3

8/8
4/4
3/3

U
U
3/3

U
U
3/3

U
4/4
3/3

U
U
3/3

U
U
3/3

                                    C-16

-------
                                   REGION 4
Bruce Wilson
Southern Earth Sciences, Inc.
P. 0. Box 160745
Mobile, AL  36616
205/476-5077
Bruce B. Ferguson
Harmon Engineering & Testing
Auburn Industrial Park
Auburn, AL  36830
205/821-9250
John H. Kilbourn
Consultant
1913 Capri Drive
Huntsville, AL  35811
James D. Ray
Chem-Ray
P. 0. Box 821
Florence, AL  35631
205/776-4345
David Kirby
Kirby Analytical
2109 20TH Street
Northport, AL  35476
205/333-9023
Mr. Harry Kreigh
Interscience, Inc.
5025 W. Grace Street
Tampa, FL  33607
813/879-8611
Marcia S.  Harvey
Thornton Laboratories
P.O.  Box 2880
Tampa, FL  33601
813/223-9702
RND 1:
RND 4:
RND 7:
RND10:
RND 1:
RND 4:
RND 7:
RND10:
RND 1:
RND 4:
RND 7:
RND10:
RND 1:
RND 4:
RND 7:
RND10:
RND 1:
RND 4:
RND 7:
RND10:
RND 1:
RND 4:
RND 7:
RND10:
RND 1:
RND 4:
RND 7:
RND10:
U
U
4/4
4/4
U
U
4/4
4/4
U
U
4/4
4/4
U
4/4
4/4
4/4
U
U
U
4/4
U
4/4
4/4
4/4
U
4/4
3/4
4/4
RND 2:
RND 5:
RND 8:
RND11:
RND 2:
RND 5:
RND 8:
RND11:
RND 2:
RND 5:
RND 8:
RND11:
RND 2:
RND 5:
RND 8:
RND11:
RND 2:
RND 5:
RND 8:
RND11:
RND 2:
RND 5:
RND 8:
RND11:
RND 2:
RND 5:
RND 8:
RND11:
U
U
4/4
4/4
U
U
N
4/4
U
U
4/4
4/4
U
4/4
4/4
4/4
U
U
U
4/4
U
4/4
4/4
4/4
U
4/4
4/4
4/4
RND
RND
RND

RND
RND
RND

RND
RND
RND

RND
RND
RND

RND
RND
RND

RND
RND
RND

RND
RND
RND

3:
6:
9:

3:
6:
9:

3:
6:
9:

3:
6:
9:

3:
6:
9:

3:
6:
9:

3:
6:
9:

U
4/4
3/3

U
4/4
3/3

U
4/4
3/3

8/8
4/4
3/3

U
U
U

7/8
4/4
3/3

8/8
4/4
3/3

                                     C-17

-------
                                   REGION 4
Joseph M. Kirchmer
Technical Services, Inc.
2471 Swan Street
Jacksonville, FL  32204
904/353-5761
Charles C. Haury, CIH
Environmental Science and Eng.,  Inc.
P. 0.  Box ESE
Gainesville, FL  32602
904/332-3318
Dr.s Honnorez/Ginsburg
Geoscience Consultants, Inc.
P. 0. Box 341366
Coral Gables, FL  33134
305/446-5801
James R. Burkhalter
Environmental Protection Systems, Inc.
7215 Pine Forest Road
Pensacola, FL  32504
904/944-0301
Robert E. Whippo
Minerological Consultant
210 Lake Hollingsworth Drive
Number 1304
Lakeland, FL  33803
Richard L. Hatfield
Me Crone Environmental Services, Inc.
5500 Oakbrook Parkway, Suite 200
Norcross, GA  30093
404/449-8461
Ion Petre
Geo-Environmental Services Inc.
3277 Roswell Rd. - Suite 711
Atlanta, GA  30305
404/257-9303
RND 1:
RND 4:
RND 7:
RND10:
RND 1:
RND 4:
RND 7:
RND10:
RND 1:
RND 4:
RND 7:
RND10:
RND 1:
RND 4:
RND 7:
RND10:
RND 1:
RND 4:
RND 7:
RND10:
RND 1:
RND 4:
RND 7:
RND10:
RND 1:
RND 4:
RNO 7:
RND10:
U
U
U
4/4
U
U
U
4/4
4/4
4/4
3/4
4/4
U
U
4/4
4/4
U
U
U
4/4
U
U
4/4
4/4
U
U
U
4/4
RND 2:
RND 5:
RND 8:
RND11:
RND 2:
RND 5:
RND 8:
RND11:
RND 2:
RND 5:
RND 8:
RND11:
RND 2:
RND 5:
RND 8:
RND11:
RND 2:
RND 5:
RND 8:
RND11:
RND 2:
RND 5:
RND 8:
RND11:
RND 2:
RND 5:
RND 8:
RN011:
U
U
4/4
4/4
U
U
U
4/4
4/4
4/4
4/4
4/4
U
U
4/4
4/4
U
U
4/4
3/4
U
4/4
4/4
4/4
U
U
4/4
4/4
RND
RND
RND

RND
RND
RND

RND
RND
RND

RND
RND
RND

RND
RND
RND

RND
RND
RND

RND
RND
RND

3:
6:
9:

3:
6:
9:

3:
6:
9:

3:
6:
9:

3:
6:
9:

3:
6:
9:

3:
6:
9:

U
U
2/3

U
U
N

8/8
4/4
3/3

U
4/4
3/3

U
U
3/3

U
4/4
3/3

U
U
3/3

                                    C-18

-------
                                   REGION 4
Mr.  Gordon LaPean
Dunn Laboratories
717 Edgehill Avenue,
Atlanta, GA  30318
404/873-6159
N.W.
Trabue D. Bryans
MacMillan Research, Ltd.
P. 0. Box 1305
Marietta, GA  30061
404/427-3101
Ms. Alice Farrar
Environmental Health Laboratory
1021 Ga. Avenue, 3rd Floor
Macon, GA  31201
912/745-4702
Donald K. Cavin
Cavin Analytical Consultants
P. 0. Box 454
Snellville, GA  30278
404/979-8838
Charles Greer
Law Engineering Testing Co.
P.O. Box 13260, Station K
Atlanta, GA  30324
404/873-4761
Kenneth P. Reed, Ph.D.
Northern Kentucky Envoronmental Service
300 Doctors Building
33 East Seventh Street
Covington, KY  41011
606/431-6224
Doug Price
McCoy & McCoy, Inc.
P.  0. Box 238
85 East Noel Avenue
Madisonville, KY  42431
502/821-7375
RND 1:
RND 4:
RND 7:
RND10:
RND 1:
RND 4:
RND 7:
RND10:
RND 1:
RND 4:
RND 7:
RND10:
RND 1:
RND 4:
RND 7:
RND10:
RND 1:
RND 4:
RND 7:
RND10:
RND 1:
RND 4:
RND 7:
RND10:
RND 1:
RND 4:
RND 7:
RND10:
U
4/4
4/4
4/4
U
U
U
4/4
U
4/4
4/4
4/4
U
U
U
U
4/4
4/4
4/4
4/4
U
U
U
3/4
U
U
4/4
4/4
RND 2:
RND 5:
RND 8:
RND11:
RND 2:
RND 5:
RND 8:
RND11:
RND 2:
RND 5:
RND 8:
RND11:
RND 2:
RND 5:
RND 8:
RND11:
RND 2:
RND 5:
RND 8:
RND11:
RND 2:
RND 5:
RND 8:
RND11:
RND 2:
RND 5:
RND 8:
RND11:
U
N
4/4
4/4
U
U
U
4/4
4/4
4/4
4/4
4/4
U
U
U
4/4
4/4
4/4
4/4
4/4
U
U
U
4/4
U
U
4/4
4/4
RND
RND
RND

RND
RND
RND

RND
RND
RND

RND
RND
RND

RND
RND
RND

RND
RND
RND

RND
RND
RND

3:
6:
9:

3:
6:
9:

3:
6:
9:

3:
6:
9:

3:
6:
9:

3:
6:
9:

3:
6:
9:

5/8
4/4
3/3

U
U
U

8/8
4/4
3/3

U
U
U

8/8
4/4
3/3

U
U
U

U
U
3/3

                                    C-19

-------
                                   REGION 4
Mr.  J. Daniel Cooper
Metro Service Laboratories
235 East Burnette Street
Louisville, KY 40208
502/635-5463
Robert C. Tussey, Jr.
Kenvirons, Inc.
452 Versailles Road
P.  0.  Drawer V
Frankfort, KY  40602
502/695-4357
David Kimbrell
Hall-Kimbrell Env-Svcs, Inc.
426 S. Lamar
Oxford, MS  38655
601/236-2020
Thomas J. Wilson
Micro-Methods
5106 Telephone Road
Pascagoula, MS  39567
601/769-7774
Dr. Corbin McGriff
Environmental Protection Systems, Inc.
P. 0. Box 20382
Jackson, MS  39209
601/922-8242
Larry Laird
Northrop Services, Inc.
Environmental Sciences
P. 0. Box 12313
RTP, NC  27709
919/549-0611
Steven L. Goode
PES, Inc.
1905 Chapel Hill Road
Durham, NC  27707
919/493-3536
RND 1:
RND 4:
RND 7:
RND10:
RND 1:
RND 4:
RND 7:
RND10:
RND 1:
RND 4:
RND 7:
RND10:
RND 1:
RND 4:
RND 7:
RND10:
RND 1:
RND 4:
RND 7:
RND10:
RND 1:
RND 4:
RND 7:
RND10:
RND I:
RND 4:
RND 7:
RND10:
U
4/4
N
4/4
U
U
4/4
4/4
U
U
4/4
4/4
U
U
4/4
4/4
U
4/4
4/4
4/4
4/4
4/4
3/4
4/4
U
U
U
U
RND 2:
RND 5:
RND 8:
RND11:
RND 2:
RND 5:
RND 8:
RND11:
RND 2:
RND 5:
RND 8:
RND11:
RND 2:
RND 5:
RND 8:
RND11:
RND 2:
RND 5:
RND 8:
RND11:
RND 2:
RND 5:
RND 8:
RND11:
RND 2:
RND 5:
RND 8:
RND11:
N
4/4
3/4
4/4
U
U
4/4
3/4
U
U
4/4
4/4
U
U
3/4
3/4
U
4/4
4/4
4/4
4/4
4/4
4/4
4/4
U
U
U
4/4
RND
RND
RND

RND
RND
RND

RND
RND
RND

RND
RND
RND

RND
RND
RND

RND
RND
RND

RND
RND
RND

3:
6:
9:

3:
6:
9:

3:
6:
9:

3:
6:
9:

3:
6:
9:

3:
6:
9:

3:
6:
9:

N
4/4
3/3

U
U
3/3

U
4/4
3/3

U
4/4
3/3

U
4/4
3/3

8/8
4/4
3/3

U
U
U

                                    C-20

-------
                                   REGION 4
Reginald C. Jordan, CIH
Envirosciences, Inc.
3120 Julian Dr.
Raleigh, NC  27604
919/876-9722
Mr. John Sheats
Quality Analytical Services
4701 Joseph Michael Court
Raleigh, NC  27606
919/851-2891
Larry Thompson
Thompson & Associates
P. 0. Box 766
Folly Beach, SC  29439
803/588-9155
Patrick H. Cooper
Industrial Insulation Co., Inc.
P.  0. Box 5312
N.  Charleston, SC  29406
803/747-3629
Richard D. Bennett
Azimuth, Inc.
188 Bridge Creek Drive
Goose Creek, SC  29445
803/797-6297
Kathy Turner
Phoenix Environmental
Box 121555
Nashville, TN  37212
615/833-1332
Corp.
RND 1:
RND 4:
RND 7:
RND10:
RND 1:
RND 4:
RND 7:
RND10:
RND 1:
RND 4:
RND 7:
RND10:
RND 1:
RND 4:
RND 7:
RND10:
RND 1:
RND 4:
RND 7:
RND10:
RND 1:
RND 4:
RND 7:
RND10:
U
U
U
4/4
U
4/4
4/4
4/4
U
U
1/4
3/4
U
U
4/4
N
U
U
U
U
U
U
U
4/4
RND 2:
RND 5:
RND 8:
RND11:
RND 2:
RND 5:
RND 8:
RND11:
RND 2:
RND 5:
RND 8:
RND11:
RND 2:
RND 5:
RND 8:
RND11:
RND 2:
RND 5:
RND 8:
RND11:
RND 2:
RND 5:
RND 8:
RND11:
U
U
U
3/4
U
4/4
4/4
4/4
U
4/4
3/4
2/4
U
N
4/4
4/4
U
U
U
4/4
U
U
U
4/4
RND
RND
RND

RND
RND
RND

RND
RND
RND

RND
RND
RND

RND
RND
RND

RND
RND
RND

3:
6:
9:

3:
6:
9:

3:
6:
9:

3:
6:
9:

3:
6:
9:

3:
6:
9:

U
U
3/3

8/8
4/4
3/3

U
N
2/3

U
4/4
3/3

U
U
U

U
U
U

                                     C-21

-------
                                   REGION 5
Cynthia Darling
Cencon
333 South Wabash Avenue
Chicago, IL  60604
- 3W
Richard Karuhn
Particle Data Laboratories, Ltd.
115 Hahn Street
Elmhurst, IL  60126
312/832-5658
Gary Kentgen
Anabestics/GK Consultants
407 West Eugenie Street
Chicago, IL  60614
312/944-3132
Dr.  Stephen Hall
American Industrial Laboratory
P.  0.  Box 627
Edwardsville, IL  62025
618/259-8776
Mr. Kirk Sweet!and
R. A.  I. Laboratories
8901 N.  Industrial Road
Peoria,  IL  61615
309/692-4422
Ms. Joan Wronski
NATLSCO
Environmental Science Laboratory, A-l
Long Grove, IL  60049
312/540-2488
Dr. Ian Stewart
McCrone Environmental Services, Inc.
2820 South Michigan Ave.
Chicago, IL  60616
312/842-7100
RND 1:
RND 4:
RND 7:
RND10:
RND 1:
RND 4:
RND 7:
RND10:
RND 1:
RND 4:
RND 7:
RND10:
RND 1:
RND 4:
RND 7:
RND10:
RND 1:
RND 4:
RND 7:
RND10:
RND 1:
RND 4:
RND 7:
RND10:
RND 1:
RND 4:
RND 7:
RND10:
U
U
U
4/4
U
U
4/4
4/4
U
U
U
U
U
2/4
2/4
3/4
U
4/4
N
4/4
U
4/4
4/4
4/4
4/4
4/4
4/4
4/4
RND 2:
RND 5:
RND 8:
RND11:
RND 2:
RND 5:
RND 8:
RND11:
RND 2:
RND 5:
RND 8:
RND11:
RND 2:
RND 5:
RND 8:
RND11:
RND 2:
RND 5:
RND 8:
RND11:
RND 2:
RND 5:
RND 8:
RND11:
RND 2:
RND 5:
RND 8:
RND11:
U
U
4/4
4/4
U
4/4
4/4
3/4
U
U
U
4/4
U
4/4
4/4
3/4
U
4/4
4/4
4/4
3/4
4/4
4/4
4/4
4/4
4/4
4/4
4/4
RND
RND
RND

RND
RND
RND

RND
RND
RND

RND
RND
RND

RND
RND
RND

RND
RND
RND

RND
RND
RND

3:
6:
9:

3:
6:
9:

3:
6:
9:

3:
6:
9:

3:
6:
9:

3:
6:
9:

3:
6:
9:

U
U
3/3

U
4/4
3/3

U
U
U

7/8
N
2/3

8/8
3/4
3/3

8/8
4/4
3/3

8/8
4/4
3/3

                                    C-22

-------
                                   REGION 5
James F.  Dallmeyer
Daily Analytical Laboratories
7807 N.  Pioneer Lane
Peoria,  IL  61615
309/692-5252
Fay Goldblatt
Fay Goldblatt Laboratories, Inc.
910 W. Clayton Street
Waukegan, IL  60085
312/249-1745
Debra Rickel
Environmental Research Group
117 North First Street
Ann Arbor, MI  48104
313/662-3104
Mark De Lisle
Industrial Hygiene Consultants
5741 Utah
Portage, MI  49002
616/382-3815
Gail Seifkin
IHI Kemron Environmental Services
32740 N. Western Highway
Farmington Hills, MI  48018
313/626-2426
Fred Ho Hash
Canton Analytical Laboratory
153 Elder Street
Ypsilanti, MI  48197
313/483-7430
Mr. Bob Lieckfield
Clayton Environmental
25711 Southfield Road
Southfield, MI  48075
313/424-8860
Consultants, Inc.
RND 1:
RND 4:
RND 7:
RND10:
RND 1:
RND 4:
RND 7:
RND10:
RND 1:
RND 4:
RND 7:
RND10:
RND 1:
RND 4:
RND 7:
RND10:
RND 1:
RND 4:
RND 7:
RND10:
RND 1:
RND 4:
RND 7:
RND10:
RND 1:
RND 4:
RND 7:
RND10:
U
U
U
4/4
4/4
4/4
4/4
4/4
U
4/4
3/4
4/4
U
U
U
4/4
U
4/4
4/4
4/4
U
U
U
4/4
4/4
4/4
4/4
4/4
RND 2:
RND 5:
RND 8:
RND11:
RND 2:
RND 5:
RND 8:
RND11:
RND 2:
RND 5:
RND 8:
RND11:
RND 2:
RND 5:
RND 8:
RND11:
RND 2:
RND 5:
RND 8:
RND11:
RND 2:
RND 5:
RND 8:
RND11:
RND 2:
RND 5:
RND 8:
RND11:
U
U
U
4/4
4/4
4/4
4/4
4/4
U
4/4
4/4
4/4
U
U
U
4/4
U
4/4
4/4
4/4
U
U
U
4/4
4/4
4/4
4/4
4/4
RND
RND
RND

RND
RND
RND

RND
RND
RND

RND
RND
RND

RND
RND
RND

RND
RND
RND

RND
RND
RND

3:
6:
9:

3:
6:
9:

3:
6:
9:

3:
6:
9:

3:
6:
9:

3:
6:
9:

3:
6:
9:

U
U
3/3

7/8
4/4
3/3

8/8
4/4
3/3

U
U
3/3

U
4/4
N

U
U
U

8/8
4/4
3/3

                                   C-23

-------
                                   REGION 5
Mr. Donald J. Larsen
The St. Paul Insurance Company
494 Metro Square Building
7th and Robert Streets
St. Paul, MN  55101
612/221-7043
Mr. Michael L. Boucher
MJH Mineralogical Consultants, Inc.
13345 Foliage Avenue
Apple Valley, MN  55124
612/432-8836
William F. Welbes
Twin City Testing & Engr Lab, Inc.
662 Cromwell Ave.
St. Paul, MN  55114
612/645-3601
Terrence Skelton
MWL8, Inc.
101 Peeaby  Lane
Wayzata, MN  55391
612/473-5531
Phillip Hayden
Pollution  Control Scientific  Inc.
6015 Manning  Road
Miamisburg, OH  45342
513/866-5908
 Mr.  Craig  Caldwell
 PIE  Associates,  Inc.
 11499  Chester Road
 Cincinnati,  OH 45246
 513/782-4700
 Mr.  Tom Eggers
 Lyle Laboratories
 1327 King Avenue
 Columbus, OH 43212
 614/488-1022
RND 1:
RND 4:
RND 7:
RND10:
RND 1:
RND 4:
RND 7:
RND10:
RND 1:
RND 4:
RND 7:
RND10:
RND 1:
RND 4:
RND 7:
RND10:
RND I:
RND 4:
RND 7:
RND10:
RND 1:
RND 4:
RND 7:
RND10:
RND 1:
RND 4:
RND 7:
RND10:
4/4
4/4
4/4
4/4
4/4
4/4
4/4
4/4
U
U
U
4/4
U
U
U
4/4
U
U
4/4
4/4
4/4
4/4
4/4
4/4
U
N
4/4
N
RND 2:
RND 5:
RND 8:
RND11:
RND 2:
RND 5:
RND 8:
RND11:
RND 2:
RND 5:
RND 8:
RND11:
RND 2:
RND 5:
RND 8:
RND11:
RND 2:
RND 5:
RND 8:
RND11:
RND 2:
RND 5:
RND 8:
RND11:
RND 2:
RND 5:
RND 8:
RND11:
4/4
4/4
4/4
4/4
4/4
4/4
4/4
4/4
U
U
U
4/4
U
U
U
3/4
U
U
4/4
4/4
4/4
4/4
3/4
4/4
U
4/4
N
4/4
RND
RND
RND

RND
RND
RND

RND
RND
RND

RND
RND
RND

RND
RND
RND

RND
RND
RND

RND
RND
RND

3:
6:
9:

3:
6:
9:

3:
6:
9:

3:
6:
9:

3:
6:
9:

3:
6:
9:

3:
6:
9:

8/8
4/4
3/3

8/8
4/4
3/3

U
U
N

U
U
3/3

U
N
3/3

8/8
4/4
3/3

6/8
4/4
3/3

                                    C-24

-------
                                    REGION  5
Richard E. Moore
American Analytical
100 Lincoln Street
Akron, OH  44308
Laboratories
S. H. Gelles
S. H. Gelles Associates
2836 Fisher Road
Columbus, OH  43204
614/276-2957
Sandra Kulik
Howard Laboratories
P. 0. Box 369
Dayton, OH  45449
513/294-6856
George L. Quisno
Bowser-Morner Testing Laboratories,  Inc.  RND 4:  U
420 Davis Avenue
P. 0. Box 51
Dayton, OH  45401
513/253-8805
Bill Zimmerlin
Z-Con Inc.
P. 0. Box 576
Vandalia, OH  45377
513/882-1226
D. R. Allenson, PhD
Analytical Services Division
Herron Testing Laboratories,
5405 E. Schaaf Road
Cleveland, OH  44131
216/524-1450
         Inc.
G.  Pfeifer
Bruce Menkel & Associates,
235 Industrial Drive
P.  0.  Box 159
Franklin, OH  45005
513/746-9300
       Inc.
RND 1:
RND 4:
RND 7:
RND10:
RND 1:
RND 4:
RND 7:
RND10:
RND 1:
RND 4:
RND 7:
RND10:
RND 1:
RND 4:
RND 7:
RND10:
RND 1:
RND 4:
RND 7:
RND10:
RND 1:
RND 4:
RND 7:
RND10:
RND 1:
RND 4:
RND 7:
RND10:
U
U
U
3/4
U
U
U
U
U
N
4/4
4/4
U
U
4/4
4/4
U
U
U
4/4
4/4
4/4
4/4
4/4
U
U
4/4
4/4
RND 2:
RND 5:
RND 8:
RND11:
RND 2:
RND 5:
RND 8:
RND11:
RND 2:
RND 5:
RND 8:
RND11:
RND 2:
RND 5:
RND 8:
RND11:
RND 2:
RND 5:
RND 8:
RND11:
RND 2:
RND 5:
RND 8:
RND11:
RND 2:
RND 5:
RND 8:
RND11:
U
U
U
4/4
U
U
U
4/4
U
N
4/4
4/4
U
U
4/4
4/4
U
U
U
4/4
3/4
4/4
4/4
4/4
U
U
4/4
4/4
RND
RND
RND

RND
RND
RND

RND
RND
RND

RND
RND
RND

RND
RND
RND

RND
RND
RND

RND
RND
RND

3:
6:
9:

3:
6:
9:

3:
6:
9:

3:
6:
9:

3:
6:
9:

3:
6:
9:

3:
6:
9:

U
U
U

U
U
U

N
4/4
3/3

U
4/4
3/3

U
U
3/3

8/8
4/4
3/3

U
4/4
3/3

                                     C-25

-------
                                   REGION 5
Robert Voborsky, Director
Parker Services, Inc.(Sentry Insurance)
1800 N.  Point Drive
Stevens Point, WI  54481
715/346-6804
Mr.  Richard Zimmerman
Wisconsin Occupational Health Laboratory RND
979 Jonathon Drive
Madison, WI  53713
608/263-8160
Ms. Carol Gannon
A&G Microscopy
P. 0.  Box 31
Arlington, WI  53911
608/635-2853
Mr. Thomas Stavros
Wausau Insurance Companies
Environmental Health Laboratory
2000 Westwood Dr.
Wausau, WI  54401
715/845-5211
RND 1:
RND 4:
RND 7:
RND10:
RND 1:
RND 4:
RND 7:
RND10:
RND 1:
RND 4:
RND 7:
RND10:
RND 1:
RND 4:
RND 7:
RND10:
U
3/4
2/4
4/4
U
4/4
4/4
N
U
4/4
4/4
4/4
4/4
4/4
4/4
4/4
RND 2:
RND 5:
RND 8:
RND11:
RND 2:
RND 5:
RND 8:
RND 11:
RND 2:
RND 5:
RND 8:
RND11:
RND 2:
RND 5:
RND 3:
RND1.1:
U
4/4
4/4
4/4
U
4/4
4/4
4/4
U
4/4
4/4
4/4
4/4
4/4
4/4
4/4
RND
RND
RND

RND
RND
RND

RND
RND
RND

RND
RND
RND

3:
6:
9:

3:
6:
9:

3:
6:
9:

3:
6:
9:

U
3/4
3/3

8/8
4/4
2/3

U
3/4
3/3

8/8
4/4
3/3

                                   C-26

-------
                                    REGION 6
Dr. Davy L. Bernard
Acadiana Research Laboratories
University of Southwestern  Louisiana
P. 0. Box 44210
Lafayette, LA  70504
Thomas E. Orr
EIRA, Inc.
P. 0. Box 6978
Metairie, LA  70009
504/469-0333
Mr. Gary C. Allen
Sunbelt Associates, Inc.
6961 Mayo Road
New Orleans, LA  70126
504/242-5026
Ms. Virginia Dugan
Albuchemist, Inc.
501 Wyoming Blvd., S.E.
Albuquerque, NM  87123
505/268-7367
William M. Kemp
Oklahoma State Dept. of Health
Post Office Box 53551
1000 NE 10th Street
Oklahoma City, OK  73152
405/271-5221
Dr. Tom White
Oklahoma City - County Health Dept.
Laboratory Health Services
921 Northeast 23rd Street
Oklahoma City, OK  73105
405/427-8651
J.  P.  Forsman
Accredited Industrial Hygienists
P.  0.  Box 18566
Houston, TX  77203
713/477-8101
RND 1:
RND 4:
RND 7:
RND10:
RND 1:
RND 4:
RND 7:
RND10:
RND 1:
RND 4:
RND 7:
RND10:
RND 1:
RND 4:
RND 7:
RND10:
RND 1:
RND 4:
RND 7:
RND10:
RND 1:
RND 4:
RND 7:
RND10:
RND 1:
RND 4:
RND 7:
RND10:
U
N
3/4
4/4
U
U
U
U
4/4
4/4
4/4
4/4
N
4/4
2/4
4/4
U
U
U
4/4
U
4/4
4/4
4/4
U
U
4/4
4/4
RND 2:
RND 5:
RND 8:
RND11:
RND 2:
RND 5:
RND 8:
RND11:
RND 2:
RND 5:
RND 8:
RND11:
RND 2:
RND 5:
RND 8:
RND11:
RND 2:
RND 5:
RND 8:
RND11:
RND 2:
RND 5:
RND 8:
RND11:
RND 2:
RND 5:
RND 8:
RND11:
U
4/4
4/4
4/4
U
U
U
4/4
3/4
4/4
4/4
4/4
4/4
4/4
4/4
4/4
U
U
U
3/4
3/4
4/4
4/4
4/4
U
U
4/4
4/4
RND
RND
RND

RND
RND
RND

RND
RND
RND

RND
RND
RND

RND
RND
RND

RND
RND
RND

RND
RND
RND

3:
6:
9:

3:
6:
9:

3:
6:
9:

3:
6:
9:

3:
6:
9:

3:
6:
9:

3:
6:
9:

U
4/4
N

U
U
U

8/8
4/4
3/3

7/8
4/4
3/3

U
U
3/3

8/8
4/4
3/3

U
U
3/3

                                   C-27

-------
                                   REGION 6
Ron McKee
McKee Env.  Hlth. Svcs.
11114 Sage Park
Houston, TX  77089
713/481-3501
Fred Blood
Radian Corporation
8500 Shoal Creek Boulevard
P. 0. Box 9948
Austin, TX  78766
512/454-4797
Larry Carroll
Law Engineering Testing Co.
5500 Guhn Road
Houston, TX  77040
Geroge Shattuck
NUS Corp.
900 Gemini
Houston, TX  77058
713/488-1810
Analytical Services Dept.
Southwestern Laboratories, Inc.
2575 Lone Star Drive
Dallas, TX  75212
214/688-0088
Mr. David McNamara
Continental Technical Services
Environmental Health Division
9742 Ski 11 man
Dallas, TX  75243
214/343-2025
RND 1:
RND 4:
RND 7:
RND10:
RND 1:
RND 4:
RND 7:
RND10:
RND 1:
RND 4:
RND 7:
RND10:
RND 1:
RND 4:
RND 7:
RND10:
RND 1:
RND 4:
RND 7:
RND10:
RND 1:
RND 4:
RND 7:
RND10:
U
U
U
3/4
U
4/4
N
N
U
U
U
4/4
U
U
U
4/4
4/4
4/4
1/4
N
4/4
2/4
4/4
4/4
RND 2:
RND 5:
RND 8:
RND11:
RND 2:
RND 5:
RND 8:
RND11:
RND 2:
RND 5:
RND 8:
RND11:
RND 2:
RND 5:
RND 8:
RND11:
RND 2:
RND 5:
RND 8:
RND11:
RND 2:
RND 5:
RND 8:
RND11:
U
U
U
4/4
U
4/4
4/4
3/4
U
U
U
3/4
U
U
U
4/4
3/4
4/4
4/4
4/4
4/4
4/4
4/4
3/4
RND
RND
RND

RND
RND
RND

RND
RND
RND

RND
RND
RND

RND
RND
RND

RND
RND
RND

3:
6:
9:

3:
6:
9:

3:
6:
9:

3:
6:
9:

3:
6:
9:

3:
6:
9:

U
U
2/3

U
4/4
3/3

U
U
3/3

U
U
3/3

8/8
4/4
3/3

6/8
4/4
3/3

                                     C-28

-------
                                   REGION  7
David Kimbrell
Hall-Kimbrell Envr Services,  Inc.
946 Tennessee
Lawrence, KS  66044
913/749-2301
Stephen E. Ascher
Wilson Laboratories
P. 0. Box 1858
Salina, KS  67402 1858
913/825-7186
Alan Kerschen
Langston Laboratories, Inc.
2005 West 103rd Terrace (B)
Leawood, KS  66206
913/341-7800
Eugene P. Scheide, Ph.D.
Environmetrics
1567 North Warson Road
St. Louis, MO  63132
314/427-0550
Gary Baird
Baird Scientific
P. 0. Box 842
Carthage, MO  64836
417/358-5567
Mr. William A. Eddie
Industrial Testing Laboratories, Inc.
2350 Seventh Blvd.
St. Louis, MO  63104
314/771-7111
Douglas Nimmo
Nimmo Microscopic Analysis
RR 2, Box 165
Salem, MO  65560
314/729-2521
RND 1:
RND 4:
RND 7:
RND10:
RND 1:
RND 4:
RND 7:
RND10:
RND 1:
RND 4:
RND 7:
RND10:
RND 1:
RND 4:
RND 7:
RND10:
RND 1:
RND 4:
RND 7:
RND10:
RND 1:
RND 4:
RND 7:
RND10:
RND 1:
RND 4:
RND 7:
RND 10:
U
U
4/4
4/4
U
U
U
U
U
U
U
4/4
U
U
U
3/4
U
U
4/4
N
4/4
3/4
3/4
4/4
U
U
4/4
4/4
RND 2:
RND 5:
RND 8:
RND11:
RND 2:
RND 5:
RND 8:
RND11:
RND 2:
RND 5:
RND 8:
RND11:
RND 2:
RND 5:
RND 8:
RND11:
RND 2:
RND 5:
RND 8:
RND11:
RND 2:
RND 5:
RND 8:
RND11:
RND 2:
RND 5:
RND 8:
RND11:
U
U
4/4
4/4
U
U
U
4/4
U
U
4/4
4/4
U
U
U
3/4
U
4/4
4/4
4/4
2/4
4/4
4/4
3/4
U
U
4/4
3/4
RND
RND
RND

RND
RND
RND

RND
RND
RND

RND
RND
RND

RND
RND
RND

RND
RND
RND

RND
RND
RND

3:
6:
9:

3:
6:
9:

3:
6:
9:

3:
6:
9:

3:
6:
9:

3:
6:
9:

3:
6:
9:

U
4/4
3/3

U
U
U

U
U
3/3

U
U
3/3

U
4/4
3/3

8/8
4/4
3/3

U
U
3/3

                                  C-29

-------
                                    REGION  7
David J. Roth                             RND 1:  U    RND 2:  U    RND 3: U
Larron Laboratory                         RND 4:  U    RND 5:  U    RND 6: U
529 Broadway                              RND 7:  U    RND 8:  4/4  RND 9: 3/3
Cape Giradeau, MO  63701                  RND10:  4/4  RND11:  4/4
314/334-8910
                                   C-30

-------
                                   REGION 8
Mr.  Todd Reynolds
Mountain Analysts Corporation
1330 Lyden Street, Suite 114
Denver, CO  80220
303/393-0945
Dr. Robert Hager, Jr.
Hager Laboratories, Inc.
4725 Paris Street
Denver, CO  80239
303/371-1441
Larry Cox
Laroratory Manager
CSMRI-Analytica
5920 Mclntyre Street
Golden, CO  80403
303/279-2581
Donna C. Mefford
DCM Science Laboratories
6617 W.  32nd Ave.
Wheatridge, CO  80033
303/232-7244
Briant L. Davis
South Dakota School of Mines & Tech
Rapid City, SD  57701-3995
605/394-2291
Daniel T. Wade
Analytica Laboratories, Inc.
208 S. Wayland Ave.
Sioux Falls, SD  57103-1791
605/338-0555
Mr. James Perkins
Utah Biomedical Test Laboratory
520 Wakara Way
Salt Lake City, UT  84108
801/581-8987
RND 1:
RND 4:
RND 7:
RND10:
RND 1:
RND 4:
RND 7:
RND10:
RND 1:
RND 4:
RND 7:
RND10:
RND 1:
RND 4:
RND 7:
RND10:
RND 1:
RND 4:
RND 7:
RND 10:
RND 1:
RND 4:
RND 7:
RND10:
RND 1:
RND 4:
RND 7:
RND10:
U
4/4
3/4
4/4
4/4
4/4
4/4
4/4
4/4
4/4
3/4
4/4
U
U
U
4/4
U
U
U
4/4
U
U
U
4/4
4/4
4/4
4/4
4/4
RND 2:
RND 5:
RND 8:
RND11:
RND 2:
RND 5:
RND 8:
RND11:
RND 2:
RND 5:
RND 8:
RND11:
RND 2:
RND 5:
RND 8:
RND11:
RND 2:
RND 5:
RND 8:
RND11:
RND 2:
RND 5:
RND 8:
RND11:
RND 2:
RND 5:
RND 8:
RND11:
U
4/4
4/4
4/4
4/4
4/4
4/4
4/4
4/4
4/4
4/4
4/4
U
U
U
4/4
U
U
U
4/4
U
U
U
4/4
4/4
4/4
4/4
4/4
RND
RND
RND

RND
RND
RND

RND
RND
RND

RND
RND
RND

RND
RND
RND

RND
RND
RND

RND
RND
RND

3:
6:
9:

3:
6:
9:

3:
6:
9:

3:
6:'
9:

3:
6:
9:

3:
6:
9:

3:
6:
9:

7/8
4/4
3/3

7/8
4/4
3/3

8/8
4/4
3/3

U
U
N

U
U
3/3

U
U
3/3

8/8
4/4
3/3

                                   C-31

-------
                                   REGION 9
Gerald J. Karches
Southwest Hazard Control, Inc.
10941 N. Coyote Lane
Tucson, AZ 85741
602/744-1060
James R. Kessler
Microprobe
5104 E. Burns
Tucson, AZ  85711
602/745-1189
Ms. Kathy Jones
Health Science Associates
10941 Bloomfield Street
Suite B/C
Los Alamitos, CA  90720
213/430-1031
Kenneth S. Cohen
Consulting Health Services
P.O. Box 1625
El Cajon, CA  92022
619/579-6233
Robert Oneill
Micro-Chem Laboratories
349 Lincoln Avenue
San Jose, CA  95126
408/993-0998
Ms. B. M. Tooper
EMS Laboratories
12563 Crenshaw Boulevard
Hawthorne, CA  90250
213/973-6694
Frederick J. Mlakar
West Coast Technical
17605 Fabrica Way
Cerritos, CA  90701
714/523-9200
Service, Inc.
RND 1:
RND 4:
RND 7:
RND10:
RND 1:
RND 4:
RND 7:
RND10:
RND 1:
RND 4:
RND 7:
RND10:
RND 1:
RND 4:
RND 7:
RND10:
RND 1:
RND 4:
RND 7:
RND10:
RND 1:
RND 4:
RND 7:
RND10:
RND 1:
RND 4:
RND 7:
RND10:
U
U
U
U
U
U
4/4
4/4
4/4
4/4
4/4
4/4
U
4/4
4/4
N
U
U
4/4
4/4
4/4
4/4
4/4
4/4
U
U
1/4
4/4
RND 2:
RND 5:
RND 8:
RND11:
RND 2:
RND 5:
RND 8:
RND11:
RND 2:
RND 5:
RND 8:
RND11:
RND 2:
RND 5:
RND 8:
RND11:
RND 2:
RND 5:
RND 8:
RND11:
RND 2:
RND 5:
RND 8:
RND11:
RND 2:
RND 5:
RND 8:
RND11:
U
U
U
4/4
U
U
4/4
4/4
4/4
4/4
4/4
4/4
U
4/4
4/4
4/4
U
U
4/4
3/4
4/4
4/4
4/4
4/4
U
U
4/4
4/4
RND
RND
RND

RND
RND
RND

RND
RND
RND

RND
RND
RND

RND
RND
RND

RND
RND
RND

RND
RND
RND

3:
6:
9:

3:
6:
9:

3:
6:
9:

3:
6:
9:

3:
6:
9:

3:
6:
9:

3:
6:
9:

U
U
U

U
4/4
3/3

8/8
4/4
3/3

8/8
4/4
3/3

U
4/4
3/3

8/8
4/4
3/3

U
4/4
3/3

                                   C-32

-------
                                   REGION 9
Mr. Brig P. Tamayo
C.E.D., Inc.
1249 Pinole Valey Road
Pinole, CA  94564
415/234-3761
Mr. D. L. Dyer
Dyer  Laboratories, Inc.
22527 Crenshaw Blvd., #209
Torrance, CA  90505
213/530-3322
Dr. Stuart Salot
Certified Testing Laboratories, Inc.
2905 East Century Boulevard
South Gate, CA  90280
213/564-2641
Mr. Michael McLara
McLara Laboratory
Asbestos Control Division
3972 Miller Way
Sacramento, CA  95817
916/451-6219
Mr. Kip Fout
EAL Corporation
2030 Wright Avenue
Richmond, CA  94804
415/235-2633
Charles W. Ay
Asbestos Detechon, Inc.
7602 Talbert Ave., Unit F
Huntington Beach, CA  92648
714/847-1873
Martin H.  Finkel
Finkel Analytical Laboratory
1750 E.  Ocean Blvd.  #1102
Long Beach, CA  90802
213/436-6544
RND 1:
RND 4:
RND 7:
RND10:
RND 1:
RND 4:
RND 7:
RND10:
RND 1:
RND 4:
RND 7:
RND10:
RND 1:
RND 4:
RND 7:
RND10:
RND 1:
RND 4:
RND 7:
RND10:
RND 1:
RND 4:
RND 7:
RND10:
RND 1:
RND 4:
RND 7:
RND10:
4/4
4/4
4/4
4/4
U
4/4
4/4
4/4
4/4
4/4
4/4
4/4
U
4/4
3/4
4/4
4/4
4/4
4/4
4/4
U
U
U
4/4
U
U
U
4/4
RND 2:
RND 5:
RND 8:
RND11:
RND 2:
RND 5:
RND 8:
RND11:
RND 2:
RND 5:
RND 8:
RND11:
RND 2:
RND 5:
RND 8:
RND11:
RND 2:
RND 5:
RND 8:
RND11:
RND 2:
RND 5:
RND 8:
RND11:
RND 2:
RND 5:
RND 8:
RND11:
4/4
4/4
4/4
4/4
U
4/4
4/4
4/4
4/4
4/4
4/4
4/4
4/4
4/4
4/4
4/4
4/4
4/4
4/4
4/4
U
U
U
4/4
U
U
4/4
4/4
RND
RND
RND

RND
RND
RND

RND
RND
RND

RND
RND
RND

RND
RND
RND

RND
RND
RND

RND
RND
RND

3:
6:
9:

3:
6:
9:

3:
6:
9:

3:
6:
9:

3:
6:
9:

3:
6:
9:

3:
6:
9:

8/8
4/4
3/3

8/8
4/4
3/3

8/8
4/4
3/3

8/8
4/4
3/3

8/8
4/4
3/3

U
U
U

U
U
3/3

                                   C-33

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                                   REGION 9
Daniel M.  Baxter
Science Applications, Inc.
476 Prospect Street
La Jolla,  CA  92038
619/456-6624
Mr. Karl Schiller
Truesdale Laboratories, Inc.
14201 Franklin Avenue
Tustin, CA  92680
213/225-1564
Dr. Jerry Tuma
Environmental Laboratory
Fireman's Fund Insurance Companies
3700 Lakeville Highway
Petaluma, CA  94952
415/929-2053
Ralph E. Allan
Med-Tox Associates, Inc.
1401 Warner Ave., Suite A
Tustin, CA  92680
714/669-0620
Dan Baxter
Environmental Testing Associates
5290 Soledad Road
San Diego, CA  92109
619/270-1249
                         Laboratories
Mr.  Shui Fong
Scientific Environmental
924 Industrial Avenue
Palo Alto, CA  94303
415/856-6011
Bonnie Lee Kellog
Taka West
663 South Bernardo Avenue, Suite 145
Sunnyvale, CA  94087
415/659-9751
RND 1:
RND 4:
RND 7:
RND10:
RND 1:
RND 4:
RND 7:
RND10:
RND 1:
RND 4:
RND 7:
RND10:
RND 1:
RND 4:
RND 7:
RND10:
RND 1:
RND 4:
RND 7:
RND10:
RND 1:
RND 4:
RND 7:
RND10:
RND 1:
RND 4:
RND 7:
RND10:
U
U
4/4
4/4
4/4
4/4
4/4
4/4
U
4/4
4/4
4/4
U
U
U
4/4
U
U
4/4
N
U
4/4
4/4
4/4
U
U
4/4
4/4
RND 2:
RND 5:
RND 8:
RND11:
RND 2:
RND 5:
RND 8:
RND11:
RND 2:
RND 5:
RND 8:
RND11:
RND 2:
RND 5:
RND 8:
RND11:
RND 2:
RND 5:
RND 8:
RND11:
RND 2:
RND 5:
RND 8:
RND11:
RND 2:
RND 5:
RND 8:
RND11:
U
U
4/4
4/4
4/4
4/4
4/4
4/4
U
4/4
4/4
3/4
U
U
U
4/4
U
U
4/4
4/4
4/4
4/4
4/4
4/4
U
4/4
4/4
4/4
RND
RND
RND

RND
RND
RND

RND
RND
RND

RND
RND
RND

RND
RND
RND

RND
RND
RND

RND
RND
RND

3:
6:
9:

3:
6:
9:

3:
6:
9:

3:
6:
9:

3:
6:
9:

3:
6:
9:

3:
6:
9:

U
4/4
3/3

8/8
4/4
3/3

U
4/4
3/3

U
U
U

U
U
3/3

8/8
4/4
3/3

U
4/4
3/3

                                     C-34

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                                    REGION  9
Mr. Fred Hertlein                         RND  1:  4/4  RND 2:  3/4  RND 3: 7/8
Industrial Analytical Laboratory,  Inc.    RND  4:  4/4  RND 5:  4/4  RND 6: 4/4
1523 Kalakaua Avenue                      RNO  7:  4/4  RND 8:  4/4  RND 9: 3/3
Suite 207                                 RND10:  4/4  RND11:  4/4
Honolulu, HI  96826
808/947-5402
                                    C-35

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                                   REGION 10
Mr. Gene Yonkin
Chemical & Geological
5633 B Street
Anchorage, AK  99502
907/279-4014
Labs of Alaska
Gerald Pi res
Northwest Testing Laboratories
4115 North Mississippi Avenue
Portland, OR  97217
503/288-7086
Gail Bohnhoff-Hlavacek
Puget Sound Microscopy
3716 SW Trenton
Seattle, WA  98126
206/932-8188
Sam LeBarron
Northwest Laboratories
1530 First Avenue South
Seattle, WA  98134
206/622-0680
Ms. Maureen Hamilton
NHS, Inc./Hanford Env. Health Foundation RNO 4:
Environmental Health Sciences Laboratory RND 7: 4/4
805 Goethals Ave.                        RND10: 4/4  RND11: 4/4
Rich!and, WA  99352
509/376-6980
RND
RND
RND
1:
4:
7:
RND10:
RND
RND
RND
1:
4:
7:
RND10:
RND
RND
RND
1:
4:
7:
RND10:
RND
RND
RND
1:
4:
7:
RND10:
RND
RND
RND
1:
4:
7:
U
4/4
3/4
4/4
U
U
3/4
4/4
U
U
4/4
4/4
U
U
U
4/4
U
4/4
4/4
RND
RND
RND
2:
5:
8:
RND11:
RND
RND
RND
2:
5:
8:
RND11:
RND
RND
RND
2:
5:
8:
RND11:
RND
RND
RND
2:
5:
8:
RND11:
RND
RND
RND
2:
5:
8:
U
4/4
4/4
3/4
U
U
4/4
4/4
U
U
4/4
4/4
U
U
U
4/4
U
4/4
4/4
RND
RND
RND

RND
RND
RND

RND
RND
RND

RND
RND
RND

RND
RND
RND
3:
6:
9:

3:
6:
9:

3:
6:
9:

3:
6:
9:

3:
6:
9:
8/8
4/4
3/3

U
4/4
N

U
4/4
3/3

U
U
U

8/8
4/4
3/3
Mr. Russel Crutcher
Microlab Northwest
7609 140th Place, N.E.
Redmond, WA  98052
206/885-9419
                   RND 1:  U
                   RND 4:  4/4
                   RND 7:  4/4
                   RND10:  4/4
RND 2:
RND 5:
RND 8:
RND11:
U
4/4
4/4
4/4
RND 3:  8/8
RND 6:  3/4
RND 9:  3/3
                                   C-36

-------
    Appendix D



Quantitative Results

-------
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  0)
                                          Number of Laboratories

              o    3     S    3    g    g     §     S     §
§     2

-------
   e-a
Number of Laboratories




               o

-------
                      35 r
O

-Pi
                      30
                                          6    8    10    12    14   16    18   20    22  24      30    35   40    45   60    70   80    90
                       Figure 3.  ftound 9 quantitative results for sample C.  TT>e sample contained  I-3JI chrysotlle,  50-60$  gypsum,  30-40$
                                  mica and <\% fibrous glass.

-------
D

cn
                 i
                 •8
                 i
                 a
                    300
                    200
                    100
                                                8   10   12    14   16

                                                   Total Percent Asbestos
                                          18    20    22   24
                     Figure 4.
Round 9 quantitative results for sample D.   The  sample contained
4-8J{ fibrous glass, <\% cellulose and  greater than  90% calcium
carbonate.

-------
     9-Q
Number of Laboratories
                                              s     g

-------
                      10   20
 30    40    50  60

Total Percent Asbestot
70   80    90   100
Figure 6.  Round 10 quantitative results for sample B.   The  sample  contained 50-60%
           chrysotlle and 40-50J cellulose.

-------
N —>_!

 s       §        §
N)
_»
O
N)


§
N>
•sj
O

-------
o
                           (O
                           c

                           d>
                    o» v in ;o
                    3 vO Ql O
                         3 c
O   — Q.
01 -t. 

O- CT O O
O T •
3 O    -Q
a c    c
-Kn H o»
 -t-

   » u> ^
   in m a
   in 3 -+
     TJ —
   o — <
   3 a> a>
   Q.
     o -i
   A O ID
                      — • 3 VI
                      O 0)
                      a> a. -*
                           O
                                           s
Number of Laboratories

            -*         _»

            8         g
                                                                 ro
ss
o

-------
o
I
                                    4      10   20   30     40   50    60   70    80   90   100


                                                  Total Percent Asbestos

                   Figure 9.   Round  11  quantitative results for sample A.  The sample contained

                               100? fibrous glass.

-------
3

2
4-
o
k_

XJ
                           10    20   30    40    50   60

                                  Total Percent Asbestos
70   80   90   100
    Figure 10.   FtounJ  !1  quantitative results for sample B.   The  sample  contained

                >98? •'•or. do lite and <2% opaques, carbonates  and  trace

                unldeiT.  .able phases.
                                       D-ll

-------
I
H-'
IN3
                                        6    8
10      20    30   40    50    60   70    80    90    100

    Total Percent Asbestos
                   Figure II.  Round  II quantitative  results for sample C.  The sample  contained >98%
                               pyrophylllte and  <2%  lime.

-------
                          270
                          240
                          210
a
 i
                       „  180
                      .£

                      8
                       S
J3
•s
i
                          150
                           120
                            90
                            60
                            30
                                0   10    20   30    40    50    60    70   80    90  100

                                                     Total Percent Asbestos

                            Figure  12.  Round 12 quantitative results  for  sample C.   The sample contained
                                        100J carbon fibers.

-------