vvEPA
              United States
              Environmental Protection
              Agency
               Office of Research and
               Development
               Washington DC 20460
 EPA/600/AP-93/004b
 December 1993
 External Review Draft
Air Quality
Criteria for
Ozone and
Related
Photochemical
Oxidants
Review
Draft
(Do Not
Cite or
Quote)
             Volume II of
                             Notice
               This document is a preliminary draft. It has not been formally
             released by EPA and should not at this stage be construed to
             represent Agency policy. It is being circulated for comment on its
             technical accuracy and policy implications.

-------
DRAFT-DO NOT QUOTE OR CITE                            EPA/600/AP-93/0041
                                                          December 1993
                                                          External Review Oral
                Air Quality Criteria for Ozone
          and  Related Photochemical Oxidants
                           Volume  II  of  III
                                    NOTICE
                  This document is a preliminary draft. It has not been formally
                  released by EPA and should not at this stage be construed to
                  represent Agency policy. It is being circulated for comment on
                  its technical accuracy and policy implications.
                                                     U.S. Environmental Protection y
                                                     •fgion 5, Library (PL-12J)
                                                     «..vVesi Jfckson Boulevard, 12i
                                                     Chicago, JL  60604-3590


                    Environmental Criteria and Assessment Office
                    Office of Health and Environmental Assessment
                        Office of Research and Development
                        U.S. Environmental Protection  Agency
                         Research Triangle Park, NC  27711
                                                       Printed on Recycled Paper

-------
                                 DISCLAIMER

     This document is an external draft for review purposes only and does not constitute
U.S. Environmental Protection Agency policy.  Mention of trade names or commercial
products does not constitute endorsement or recommendation for use.
December 19P3                        H-ii      DRAFT-DO NOT QUOTE OR CITE

-------
                                      PREFACE

     In 1971, the U.S. Environmental Protection Agency (EPA) promulgated National
Ambient Air Quality Standards (NAAQS) to protect the public health and welfare from
adverse effects of photochemical oxidants.  In 1979, the chemical designation of the
standards was changed from photochemical oxidants to ozone (O3).  This document,
therefore, focuses primarily on the scientific air quality criteria for O3 and, to a lesser extent,
for other photochemical oxidants like hydrogen peroxide and the peroxyacyl nitrates.
     The EPA promulgates the NAAQS on the basis of scientific information contained in
air quality criteria documents.  The previous O3  criteria document, Air Quality Criteria for
Ozone and Other Photochemical Oxidants,  was released in August 1986  and a supplement,
Summary of Selected New Information on Effects of Ozone on Health and Vegetation, was
released in January  1992.  These documents were used as the basis for a March 1993
decision by EPA that revision of the existing 1-h NAAQS for O3 was not appropriate at that
time. That decision, however, did not take into  account some of the newer scientific data
that became available after completion of the 1986 criteria document.  The purpose of this
revised air quality criteria document for O3 and related photochemical oxidants is to  critically
evaluate and assess the latest scientific data associated with exposure to the concentrations of
these pollutants found in ambient air.  Emphasis is placed on the presentation of health and
environmental effects data; however, other scientific data are presented and evaluated in
order to provide a better understanding of the nature,  sources, distribution, measurement,
and concentrations of O3 and related photochemical oxidants and their precursors in the
environment.  Although the document is not intended  to be an exhaustive literature review, it
is intended to cover all pertinent literature available through  the end of 1993.
      This document was prepared and peer reviewed  by experts from various state and
Federal governmental offices, academia, and private industry for use by  EPA to support
decision making regarding potential  risks to public health and welfare. The Environmental
Criteria and Assessment Office of EPA's Office of Health and Environmental Assessment
acknowledges with appreciation the contributions provided by these authors and reviewers as
well as the diligence of its staff and  contractors in  the preparation of this document at the
request of the Office of Air Quality  Planning and Standards.

December 1993                           H-iii       DRAFT-DO NOT QUOTE OR CITE

-------
                   Air Quality Criteria for Ozone
                 and Other Photochemical Oxidants
                       TABLE OF CONTENTS

                             Volume I

1.  EXECUTIVE SUMMARY 	      1-1

2.  INTRODUCTION	      2-1

3.  TROPOSPHERIC OZONE AND ITS PRECURSORS	      3-1

4.  ENVIRONMENTAL CONCENTRATIONS, PATTERNS, AND
   EXPOSURE ESTIMATES	      4-1


                            Volume n

5.  ENVIRONMENTAL EFFECTS OF OZONE AND
   RELATED PHOTOCHEMICAL OXIDANTS	      5-1

APPENDIX 5A:  COLLOQUIAL AND LATIN NAMES  	      5A-1


                            Volume HI

6.  TOXICOLOGICAL EFFECTS OF OZONE AND RELATED
   PHOTOCHEMICAL OXIDANTS	      6-1

7.  HUMAN HEALTH EFFECTS OF OZONE AND RELATED
   PHOTOCHEMICAL OXIDANTS	      7-1

8.  EXTRAPOLATION OF ANIMAL TOXICOLOGICAL DATA
   TO HUMANS	      8-1

9.  INTEGRATIVE SUMMARY OF OZONE HEALTH EFFECTS 	      9-1

APPENDIX A:  GLOSSARY OF TERMS AND SYMBOLS  	      A-l
December 1993                    H-v     DRAFT-DO NOT QUOTE OR CITE

-------
                             TABLE OF CONTENTS
                                                                        Page

LIST OF TABLES  	       Il-xi
LIST OF FIGURES	       II-xv
AUTHORS, CONTRIBUTORS, AND REVIEWERS  	       H-xix
U.S. ENVIRONMENTAL PROTECTION AGENCY PROJECT TEAM
FOR DEVELOPMENT OF AIR QUALITY CRITERIA FOR OZONE
AND RELATED PHOTOCHEMICAL OXIDANTS	       H-xxiii
5.  ENVIRONMENTAL EFFECTS OF OZONE AND RELATED
    PHOTOCHEMICAL OXIDANTS	     5-1
    5.1   INTRODUCTION  	     5-1
    5.2   METHODOLOGIES USED IN VEGETATION RESEARCH  ...     5-6
          5.2.1    Fumigation Systems	     5-6
                  5.2.1.1  Methodologies Discussed in the Air Quality
                         Criteria for Ozone and Other Photochemical
                         Oxidants (1986)	     5-7
                  5.2.1.2  Methodologies Referenced Since the Air
                         Quality Criteria for Ozone and Other
                         Photochemical Oxidants (1986)  	     5-9
                  5.2.1.3  Flux Measurement	     5-10
          5.2.2    Experimental Design and Data Analysis  	     5-16
          5.2.3    Mechanistic Process Models  	     5-19
    5.3   SPECIES RESPONSE/MODE OF ACTION	     5-20
          5.3.1    Introduction  	     5-20
          5.3.2    Ozone Uptake  	     5-22
                  5.3.2.1  Ozone Uptake by Plant Canopies	     5-22
                  5.3.2.2  Ozone Absorption by Leaves	     5-25
          5.3.3    Resistance Mechanisms  	     5-29
                  5.3.3.1  Stomatal Limitation  	     5-29
                  5.3.3.2  Detoxification	     5-30
          5.3.4    Physiological Effects of Ozone	     5-31
                  5.3.4.1  Carbohydrate Production and Allocation	     5-35
                  5.3.4.2  Compensation	     5-37
          5.3.5    Role of Age  and Size Influencing Response to Ozone  . .     5-38
                  5.3.5.1  Summary	     5-41
    5.4   FACTORS THAT MODIFY PLANT RESPONSE  	     5-43
          5.4.1    Modification of Functional and Growth Responses ....     5-43
          5.4.2    Genetics	     5-44
          5.4.3    Environmental Biological Factors  	     5-57
                  5.4.3.1  Oxidant-Plant-Insect Interactions  	     5-59
                  5.4.3.2  Oxidant-Plant-Pathogen Interactions  	     5-63
                  5.4.3.3  Oxidant-Plant-Symbiont Interactions  	     5-68
December 1993                        H-vii     DRAFT-DO NOT QUOTE OR CITE

-------
                         TABLE OF CONTENTS (cont'd)
                                                                       Page

                  5.4.3.4 Oxidant-Plant-Plant Interactions-
                         Competition  	    5-69
          5.4.4    Physical Factors	    5-71
                  5.4.4.1 Light	    5-71
                  5.4.4.2 Temperature	    5-73
                  5.4.4.3 Humidity and Surface Wetness  ..........    5-75
                  5.4.4.4 Drought and Salinity .,....„„,.„„	    5-76
          5.4.5    Nutritional Factors	    5-82
          5.4.6    Interactions with Other Pollutants 	    5-84
                  5.4.6.1 Oxidant Mixtures	    5-85
                  5.4.6.2 Sulfur Dioxide	    5-85
                  5.4.6.3 Nitrogen Dioxide	    5-88
                  5.4.6.4 Hydrogen Fluoride and Other Gaseous
                         Pollutants  	    5-91
                  5.4.6.5 Acid Deposition  	    5-92
                  5.4.6.6 Heavy Metals	    5-96
                  5.4.6.7 Mixtures of Ozone with Two or More
                         Pollutants  	    5-97
          5.4.7    Interactions with Agricultural Chemicals	    5-97
          5.4.8    Factors Associated with Global Climate Change  	    5-99
          5.4.9    Summary	    5-103
    5.5    EFFECTS-BASED AIR QUALITY EXPOSURE INDICES ....    5-106
          5.5.1    Introduction	    5-106
                  5.5.1.1 Biological Support for Identifying Relevant
                         Exposure Indices	    5-106
                  5.5.1.2 Historical Perspective on Developing Exposure
                         Indices	  .    5-108
          5.5.2    Developing Exposure Indices   	    5-114
                  5.5.2.1 Experimental Design and Statistical Analysis  ..    5-114
                  5.5.2.2 Studies with Two or More Different Patterns
                         of Exposure   	    5-119
                  5.5.2.3 Combinations of Years, Sites, or Species:
                         Comparisons of Yield Losses with Different
                         Exposure Durations  	    5-123
                  5.5.2.4 Comparisons of Measures of Exposure Based
                         on Reanalysis of Single-Year, Single-Species
                         Studies	    5-136
          5.5.3    Summary	    5-151
    5.6    EXPOSURE-RESPONSE OF PLANT SPECIES	    5-154
          5.6.1    Introduction  	    5-154
          5.6.2    Summary  of Conclusions from the Previous Criteria
                  Documents	    5-155
          5.6.3    Information in the Published Literature Since 1986 ....    5-161
December 1993                        H-viii     DRAFT-DO NOT QUOTE OR CITE

-------
                          TABLE OF CONTENTS (cont'd)
                                                                         Page

                  5.6.3.1  Effects of Ozone on Short-Lived (Less Than
                          One-Year) Species	     5-164
          5.6.4   Effects of Ozone on Long-Lived Plants	     5-184
                  5.6.4.1  Perennial Agricultural Crops	     5-185
                  5.6.4.2  Effects of Ozone on Deciduous Shrubs
                          and Trees  	     5-187
                  5.6.4.3  Effects of Ozone on Evergreen Trees   	     5-200
          5.6.5   Assessments Using Ethylene Diurea as a Protectant  . . .     5-208
          5.6.6   Summary	     5-213
    5.7   EFFECTS OF OZONE ON NATURAL ECOSYSTEMS	     5-215
          5.7.1   Introduction  	     5-215
          5.7.2   Ecosystem Characteristics	     5-216
                  5.7.2.1  Expected Sequence of Events   	     5-216
          5.7.3   Ecosystem Response to Stress   	     5-219
                  5.7.3.1  Forest Ecosystems	     5-219
                  5.7.3.2  The San Bernardino Forest Ecosystem—
                          Before 1986	     5-223
                  5.7.3.3  The San Bernardino Forest Ecosystem—
                          Since 1986	     5-229
                  5.7.3.4  The Sierra Nevada Mountains	     5-231
                  5.7.3.5  The Appalachian Mountains—Before 1986  . . .     5-234
                  5.7.3.6  The Appalachian Mountains—Since 1986  ....     5-235
                  5.7.3.7  Foliage and Soil-Mediated Effects—Combined
                          Stress   	     5-237
                  5.7.3.8  Mycorrhizae-Plant Interactions	     5-242
                  5.7.3.9  Rhizosphere and Soil Processes	     5-246
          5.7.4   Summary	     5-248
    5.8   EFFECTS OF OZONE ON AGRICULTURE, FORESTRY, AND
          ECOSYSTEMS:  ECONOMICS	     5-250
          5.8.1   Introduction  	     5-250
          5.8.2   Agriculture	     5-251
                  5.8.2.1  Review of Key Studies from the 1986
                          Document  	     5-252
                  5.8.2.2  A Review of Post-1986 Assessments	     5-256
                  5.8.2.3  Limitations and  Future Research Issues  	     5-258
          5.8.3   Forests (Tree Species)  	     5-259
          5.8.4   Valuing Ecosystem Service Flows	     5-262
                  5.8.4.1  Background  	     5-262
                  5.8.4.2  The Economic Perspective	     5-263
                  5.8.4.3  Nonmarket Valuation:  Implications for
                          Ecosystem Service Flows	     5-265
                  5.8.4.4  Challenges in  Linking Valuation Techniques
                          to Ecosystem Service Flows	     5-269
                  5.8.4.5  The Research  Agenda	     5-271

December 1993                          H-ix      DRAFT-DO NOT QUOTE OR CITE

-------
                          TABLE OF CONTENTS (cont'd)
                                                                       Page

                  5.8.4.6 Valuing Ecosystem Service Flows:
                         Summary	    5-273
          5.8.5    Summary	    5-274
    5.9    INTEGRATIVE SUMMARY AND CONCLUSIONS FOR
          VEGETATION AND ECOSYSTEM EFFECTS	     5-275
          5.9.1    Introduction  	    5-275
          5.9.2    Species Response and Ecosystem Response  	     5-276
          5.9.3    How Does Ozone Affect Plants?	     5-278
          5.9.4    Factors That Modify Plant Response to Ozone  	     5-280
                  5.9.4.1 Genetics 	    5-280
                  5.9.4.2 Environmental Factors	     5-281
          5.9.5    Exposure Dynamics   	    5-283
          5.9.6    What Measure of Exposure Characterizes Species
                  Effects?	    5-284
          5.9.7    What Is the Estimated Crop Yield or Biomass Change
                  with Ozone Exposure?	    5-286
          5.9.8    Ozone Concentration Across the United States  	     5-287
          5.9.9    What Are the Exposure Effects on Other Species—Trees
                  and Ornamentals?	    5-290
          5.9.10   Spatial Characterization of Ozone Effects  	     5-292
          5.9.11   What Is the Effect of Ozone on Ecosystems?  	     5-305
          5.9.12   Economic Assessments	     5-310
    5.10  EFFECTS OF OZONE ON MATERIALS  	     5-311
          5.10.1   Introduction  	    5-311
          5.10.2   Mechanisms of Ozone Attack and Antiozonant
                  Protection	    5-311
                  5.10.2.1  Elastomers  	    5-311
                  5.10.2.2  Textile Fibers and Dyes	     5-314
                  5.10.2.3  Paint	    5-316
          5.10.3   Exposure-Response Data  	    5-316
                  5.10.3.1  Elastomer Cracking	    5-317
                  5.10.3.2  Dye Fading	    5-325
                  5.10.3.3  Fiber Damage  	    5-334
                  5.10.3.4  Paint Damage  	    5-338
                  5.10.3.5  Cultural Properties Damage	     5-341
          5.10.4   Economics  	    5-344
                  5.10.4.1  Introduction	    5-344
                  5.10.4.2  Methods of Cost Classification and
                           Estimation  	    5-345
                  5.10.4.3  Aggregate Cost Estimates	    5-346
          5.10.5   Summary and Conclusions	    5-348
    REFERENCES	    5-352

APPENDIX 5A: COLLOQUIAL AND LATIN NAMES   	    5A-1

December 1993                          n-x      DRAFT-DO NOT QUOTE OR CITE

-------
                                LIST OF TABLES
Number

5-1      Examples of Intraspecific Variation of Foliar Symptoms in
         Ozone Response  ..................	       5-45

5-2      Examples of Intraspecific Variation in Growth Responses
         Following Ozone Exposures	       5-47

5-3      Mortality of Three Ozone Sensitivity Classes of Eastern
         White Pine  (Pinus strobus L.) Trees During the Period
         from  1971 to 1986	       5-53

5-4      Examples of Ozone Effects on Pollen Germination and Tube
         Elongation	       5-56

5-5      Ozone Effects on Insect Pests	       5-60

5-6      Ozone-Plant-Pathogen Interactions  	       5-64

5-7      Field  Studies of Ozone-Drought Stress Interactions in Crop
         Species	       5-77

5-8      Ozone-Soil Nutrient Interactions  	       5-83

5-9      Some Statistical Models of Combined Ozone and Sulfur Dioxide
         Responses	       5-89

5-10     References to Reports of Interaction or No Interaction Between
         Ozone and Acid Rain or Acid Fog	       5-93

5-11     A Summary of Studies Reporting the Effects of Ozone for Two or
         More  Exposure Patterns on the Growth, Productivity, or Yield
         of Plants	       5-120

5-12     A Summary of Studies Reporting the Effects of Ozone on the
         Growth, Productivity, or Yield of Plants for Two or More
         Replicate Studies Having Equal Total Exposures and Either
         Varying Durations or Similar Durations	       5-125

5-13     Summary of Ozone Exposures That Are Closest to Those
         Predicted for 20% Yield Reduction per SUM06 Exposure
         Response Models Used by Lee et al. (1991) in Selected
         NCLAN Experiments  ............................       5-138
December 1993                         rj-xi      DRAFT-DO NOT QUOTE OR CITE

-------
                             LIST OF TABLES (cont'd)

Number                                                                   Page

5-14     Summary of Percentiles for Ozone Monitoring Sites in
         1989 (April Through October) with a Maximum
         Three-Month SUM06 Value Less Than 24.4 ppm-Hour but
         with Second Hourly Maximum Concentration  Greater Than
         or Equal to 0.125 ppm	       5-141

5-15     Summary of Percentiles for Ozone Monitoring Sites in
         1989 (April Through October) with a Maximum
         Three-Month SUM06 Value Greater Than or Equal to
         24.4 ppm-Hour but with Second Hourly Maximum
         Concentration Less Than 0.125 ppm	       5-142

5-16     Estimates of the Parameters for Fitting the Weibull
         Model Using the Seven-Hour Seasonal Mean Ozone
         Concentrations 	       5-159

5-17     Summary of Ozone Exposure Indices Calculated for
         Three- or Five-Month Growing Seasons from  1982 to 1991	       5-163

5-18     Comparison of Exposure-Response Curves Calculated
         Using the Three-Month, 24-Hour SUM06 Values for 54 NCLAN
         Cases	       5-165

5-19     Comparison of Exposure-Response Curves Calculated
         Using the 24-Hour W126 Values for 54 NCLAN Cases	       5-168

5-20     The Exposure Levels (Using Various Indices) Estimated
         to Cause at Least 10% Crop Loss in 50 and 75% of
         Experimental Cases  	       5-172

5-21     SUM06 Levels Associated  with 10 and 20% Yield Loss for
         50 and 75% of the NCLAN Crop Studies	       5-173

5-22     A Summary of Studies Reporting the Effects of Ozone
         on the Growth, Productivity, or Yield of Annual
         Plants Published Since U.S. Environmental
         Protection Agency (1986)	       5-176

5-23     A Summary of Studies Reporting the Effects of Ozone
         on the Growth, Productivity, or Yield of Perennial
         Crop  Plants Published Since U.S. Environmental
         Protection Agency (1986)	       5-188
December 1993                         H-xii     DRAFT-DO NOT QUOTE OR CITE

-------
                              LIST OF TABLES (cont'd)

Number                                                                       Page

5-24      A Summary of Studies Reporting the Effects of Ozone on the
          Growth or Productivity of Deciduous Shrubs and Trees
          Published Since U.S. Environmental Protection Agency
          (1986)	       5-192

5-25      Exposure-Response Equations That Relate Total Biomass
          (Foliage, Stem, and Root) to 24-Hour SUM06 Exposures
          Adjusted to 92 Days	       5-196

5-26      SUM06  Levels Associated with 10 and 20% Total Biomass
          Loss for 50 and 75% of the Seedling Studies	       5-198

5-27      A Summary of Studies Reporting the Effects of Ozone on the
          Growth or Productivity of Evergreen Trees Published Since
          U.S. Environmental Protection Agency (1986)	       5-201

5-28      Effects of Ethylenediurea on Ozone Responses	       5-210

5-29      Properties  of Ecological Systems Susceptible to Ozone at
          Four Levels of Biological Organization  	       5-221

5-30      San Bernardino Forest—Status 1972	       5-224

5-31      Ecosystem Response to Pollutant Stress	       5-228

5-32      Interactions of Ozone and Forest Tree Ectomycorrhizae
          Interactions  	       5-243

5-33      Recent Studies of the Economic Effects of Ozone and
          Other Pollutants on Agriculture	       5-254

5-34      Studies of the Economic Effects of Ozone and Other
          Pollutants on Forests   	       5-261

5-35      Laboratory and Field Studies on Effects of Ozone
          on Elastomers	       5-318

5-36      Protection of Tested Rubber Materials	       5-321

5-37      Effect of Ozone and Humidity on Interply Adhesion	       5-324
December 1993                         H-xiii      DRAFT-DO NOT QUOTE OR CITE

-------
                            LIST OF TABLES (cont'd)

Number                                                                 Page

5-38     Laboratory and Field Studies of the Effects of Ozone
         on Dye Fading	      5-326

5-39     Laboratory and Field Studies of the Effects of Ozone
         on Fibers	      5-335

5-40     Laboratory and Field Studies of the Effects of Ozone
         on Architectural/Industrial Paints and Coatings	      5-339

5-41     Laboratory Studies of the Effects of Ozone on Artists'
         Pigments and Dyes .	      5-342

5-42     Summary of Damage Costs to Materials by Oxidants	      5-347
 December 1993                        H-xiv      DRAFT-DO NOT QUOTE OR CITE

-------
                                  LIST OF FIGURES

Number                                                                        Page

5-1       Leaf absorption and possible functional changes that may occur
          within the plant	       5-3

5-2       Uptake of ozone from the atmosphere	       5-23

5-3       Movement of gases into and out of leaves is controlled primarily
          by the stomata—small openings in the leaf surface whose aperture
          is controlled by two guard cells	       5-26

5-4       Simulation of the effects of diurnal variation in stomatal aperture
          and in ozone concentration on ozone uptake  	       5-28

5-5       Effects of ozone absorption into a leaf	       5-32

5-6       Effect of ozone on plant function and growth	       5-34

5-7       The average injury index for visible foliar injury after exposure of
          one-year-old seedlings to 50 pphm ozone for 7.5 hours	       5-49

5-8       Frequency distribution showing the variability in ozone response
          (midpoint of whole-plant biomass)  within one half-sib family
          of loblolly pine (P. taeda L.) exposed to increasing levels
          of ozone under chronic-level field conditions over several
          growing seasons (Adams et al., 1988)	       5-50

5-9       Distribution pattern showing the number of ozone concentrations
          within specified ranges for the 1983 winter  wheat proportional
          addition experiment for the 1.4 x ambient air; 1.8 x
          ambient air treatments; and for San Bernardino, California
          in 1987	       5-118

5-10      Comparison of the Weibull exposure-response functions and its
          predicted relative yield loss curves using M-7 and daytime
          SUM06 for replicate years of National Crop Loss Assessment
          Network Program's data for cotton (var. Acala SJ-2), wheat
          (var. Vona), kidney bean  (var. California light red), and
          potato (var. Norchip), respectively	       5-129
December 1993                           H-xv      DRAFT-DO NOT QUOTE OR CITE

-------
                              LIST OF FIGURES (cont'd)

Number                                                                       Page

5-11      Predicted relative yield losses (lint weight) for Acala SJ-2
          cotton for four sites and multiple years (1981, 1982, 1988,
          1989) relative to 0.10 ppm for M7, 0.035 ppm for 2ndHDM,
          0 ppm-hour for SIGMOID, and 0 ppm-hour for SUM06, which
          correspond to typical levels in the CF chambers	       5-131

5-12      Relative effect of ozone on growth and yield of spring wheat
          cultivars (var. Star and Turbo) from two growing seasons	       5-132

5-13      Weibull exposure-response curves for the relative effect of
          ozone on grain yield of spring wheat for three years,
          individually and combined	       5-133

5-14      Quadratic exposure-response curves for the relative effect of
          ozone on grain yield of spring wheat in 1989 and 1990 using
          four different exposure indices  	       5-135

5-15      Percent reduction in net photosynthesis of pines (including
          one point for red spruce) and agricultural crops in relation
          to total ozone exposure for several ranges of peak
          concentrations	       5-144

5-16      Percent reduction in net photosynthesis and biomass growth of
          coniferous species in relation to total exposure  and estimated
          total ozone uptake	       5-145

5-17      Percent reduction in net photosynthesis and biomass growth of
          hardwood species in relation to total exposure and
          estimated total ozone uptake	       5-146

5-18      Percent reduction in net photosynthesis and biomass growth of
          agricultural crops in relation to total exposure and
          estimated total ozone uptake	       5-147

5-19      Percent reduction in biomass growth  of tree seedlings in
          relation to total exposure	       5-148

5-20      Reduction in volume production of loblolly pine seedlings
          (family 91) in relation to four exposure indices  	       5-149
December 1993                          n-xvi      DRAFT-DO NOT QUOTE OR CITE

-------
                              LIST OF FIGURES (cont'd)

Number                                                                       Page

5-21      A comparison between the resulting cumulative frequencies
          for the exposure parameters sum of all hourly average
          concentrations and the sigmoidally weighted integrated
          exposure index, W126  	       5-150

5-22      Box-plot distribution of biomass loss predictions from Weibull
          and linear exposure-response models that relate biomass and
          ozone exposure as characterized by the 24-hour SUM06 statistic
          using data from 31  crop studies from the National Crop
          Loss Assessment Network program and 26 tree seedling
          studies conducted at the Environmental Research  Laboratory
          in Corvallis, Oregon; Smoky Mountain National Park, Tennessee;
          Michigan; Ohio;  and Alabama	       5-175

5-23      Effects of ozone on plant  function and growth	       5-220

5-24      Effects of environmental stress on forest trees are presented
          on a hierarchial scale for the leaf, branch, tree, and strand
          levels of organization	       5-222

5-25      Total basal area for each species as percent of the total basal
          area for all  species in 1974 and 1988 on plots with  severe
          to moderate damage, plots with slight damage, and  plots with
          very slight damage or no  visible symptoms	       5-230

5-26      Impact of a reduced supply of carbon  to the shoot,  or
          water and nitrogen to the  roots, on subsequent
          allocation of carbon	       5-241

5-27      Regions of the United States for analysis of trends of ozone
          concentration  	       5-288

5-28      Ten-year trends in three-month SUM06 values by region at rural
          monitoring sites	       5-288

5-29      Ten-year trends in five-month 24-hour SUM06 values by region at
          rural monitoring  sites	       5-289

5-30      Ten-year trends in second highest daily maximum values by
          region  at rural  monitoring sites   	       5-289

5-31      1988 ozone monitoring site locations and calculated three-month
          SUM06 at each site 	       5-294

December 1993                          pj-xvii      DRAFT-DO NOT QUOTE OR CITE

-------
                              LIST OF FIGURES (cont'd)

Number                                                                       Page

5-32      Estimated ozone exposure across the eastern half of the
          United States for 1988 and 1989  	       5-295

5-33      Second highest daily maximum for 1989 and 1988 estimated
          across crop growing regions in the eastern half of the country  .  . .       5-296

5-34      Estimated relative yield loss for all crops from NCLAN
          database across crop growing regions of the eastern half of the
          United States in 1989 and 1988	       5-297

5-35      Estimated relative yield loss in  1988 for soybean and
          wheat from NCLAN database across crop growing regions
          of the eastern half of the United States in 1989 and 1988	       5-298

5-36      Variation in biomass reduction with year-to-year exposure
          variation	       5-299

5-37      Estimated biomass reduction for black cherry and red maple
          with 1988 ozone exposure  	       5-300

5-38      Estimated relative biomass reduction for loblolly pine
          and eastern white pine with  1988 ozone exposure   	       5-301

5-39      Box-plots of annual area-weighted yield reduction for the four
          major agronomic crop species and all crops from NCLAN with
          estimated 1988 and 1989 ozone exposure	       5-303

5-40      Box-plots of annual area-weighted biomass reduction for
          the  eight tree species with estimated 1988 and 1989 ozone
          exposure	       5-304

5-41      Postulated mechanism  for damage to elastomers by ozone	       5-313

5-42      Reaction of anthraquinone dyes with ozone and  with nitrogen
          oxides  	       5-315

5-43      Relative decrease in stress with time as a function of ozone
          concentration for polyisoprene vulcanizate  	       5-321

5-44      Relaxation  of rubber compounds in ozone is affected by the
          combination of rubber formulation and type of ozone protection  .  .       5-323
 December 1993                         n-xviii     DRAFT-DO NOT QUOTE OR CITE

-------
                  AUTHORS, CONTRIBUTORS, AND REVIEWERS

              CHAPTER 5. ENVIRONMENTAL EFFECTS OF OZONE
                  AND RELATED PHOTOCHEMICAL OXIDANTS

Principal Authors

Dr. Richard M. Adams—Department of Agriculture and Resource Economics, Oregon State
University, Corvallis, OR 97331

Dr. Christian Andersen—Environmental Research Laboratory, U.S. Environmental Protection
Agency, 200 SW 35th Street, Corvallis, OR 97333

Dr. J.H.B. Garner—Environmental Criteria and Assessment Office (MD-52),
U.S. Environmental Protection Agency, Research Triangle Park, NC  27711

Dr. Beverly A. Hale—Department of Horticultural Science, University of Guelph, Guelph,
Ontario, NIG  2W1, Canada

Dr. William E. Hogsett—Environmental Research Laboratory, U.S. Environmental Protection
Agency, 200 SW 35th Street, Corvallis, OR 97333

Dr. David F. Karnosky—School of Forestry and Wood Products, Michigan Technological
University, Houghton, MI 49931

Dr. John Laurence—Boyce Thompson Institute for Plant Research at Cornell University,
Tower Road, Ithaca, NY 14853

Dr. E. Henry  Lee—ManTech Environmental Technology, Inc., 1600 W. Western Boulevard,
Corvallis, OR 97333

Dr. Allen S. Lefohn—A.S.L. & Associates, 111 Last Chance Gulch, Suite 4A,
Helena,  MT  59601

Dr. Paul Miller—Pacific Southwest Forest and Range Experiment Station, USDA-Forest
Service Fire Lab, 4955 Canyon Crest Dr., Riverside, CA  92507

Mr. Doug Murray—TRC Environmental Corporation, 5 Waterside Crossing,
Windsor, CT  06095

Dr. Victor Runeckles—Department of Plant Science, University of British Columbia,
Vancouver, British Columbia, V6T 1Z4, Canada
December 1993                        n-xix     DRAFT-DO NOT QUOTE OR CITE

-------
              AUTHORS, CONTRIBUTORS, AND REVIEWERS (cont'd)
Dr. James A. Weber—Environmental Research Laboratory, U.S. Environmental Protection
Agency, 200 SW 35th Street, Corvallis, OR  97333

Dr. Ruth D.  Yanai—Boyce Thompson Institute for Plant Research at Cornell University,
Tower Road, Ithaca, NY 14853
Reviewers

Ms. Vicki Atwell—U.S. Environmental Protection Agency, OAQPS MD-R,
Research Triangle Park, NC 27711

Dr. Glen R. Cass—Environmental Engineering Science Department, Mail Code 138-78,
California Institute of Technology, Pasadena, CA 91125

Dr. Arthur Chapelka—Auburn University School of Forestry, Auburn, AL 36849-4201

Dr. Robert Goldstein—Electric Power Research Institute, 3412 Hillview Ave.,
Palo Alto, CA 94303

Dr. Marcia Gumpertz—Department of Statistics, North Carolina State University,
Raleigh, NC  27695

Dr. Allen Heagle—U.S. Department of Agriculture, ARS, 1505 Varsity Drive,
Raleigh, NC  27606

Dr. Robert Heath—Dept. of Botany and Plant Science, University of California,
Riverside, CA 92521

Dr. Thomas M. Hinckley—School of Forest Resources, University of Washington,
Seattle, WA  98195

Dr. Robert Kohut—Boyce Thompson Institute, Cornell University, Tower Road,
Ithaca, NY  14853-1801

Dr. Virginia Lesser—Department of Statistics, Oregon State University, Corvallia, OR  97333

Dr. Fred Lipfert—23 Carll Ct., Northport, NY  11768

Dr. Patrick McCool—SAPRC, University of California, Riverside, CA 92521

Dr. Delbert McCune—Boyce Thompson Institute, Cornell University, Tower Road,
Ithaca, NY  14853-1801
 December 1993                         H-xx      DRAFT-DO NOT QUOTE OR CITE

-------
               AUTHORS, CONTRIBUTORS, AND REVIEWERS (cont'd)
 Dr. Robert Musselman—U.S. Department of Agriculture, Forestry Service, Rocky Mountain
 Experiment Station, 240 West Prospect Road, Fort Collins, CO  80526

 Dr. Eva Pell—Pennsylvania State University, Department of Plant Pathology, 321 Buckhout
 Laboratory, University Park, PA 16802

 Dr. Phillip Rundel—Laboratory of Biomedical and Environmental Science, University of
 California, LA, 900 Veterans Ave., Los Angeles, CA 90024

 Dr. Jayson Shogren—School of Forestry and Environmental Studies, Yale University,
 New Haven, CT 06511

 Dr. James Shortle—Department of Agricultural Economics, Pennsylvania State University,
 Armsby Building, 208C, University Park, PA 16802-5502

 Dr. John Skelly—Pennsylvania State University, 108 Buckhout Laboratory,
 University Park, PA  16802

 Dr. Boyd Strain—Department of Botany, 136 Biology Science Building, Duke University,
 Durham, NC   27708

 Dr. George E. Taylor, Jr.—Biological Sciences Center, Desert Research Institute,
 7010 Dandini Blvd., Reno, NV  89512

 Dr. Patrick Temple—Statewide Air Pollution Research Center, University  of California,
 Riverside, CA 92521-0312

 Dr. David Tingey—U.S. Environmental Protection Agency, Environmental Research
 Laboratory, 200 SW 35th Street, Corvallis, OR 97333

 Dr. Michael Unsworth—Department of Atmospheric Sciences, Oregon State University,
 Corvallis, OR  97333

 Dr. David Weinstein—Boyce Thompson Institute, Cornell University, Tower Road,
 Ithaca, NY 14853-1801

 Dr. John Yocom, 12 Fox Den Road, West Simsbury, CT  06092
December 1993                          D-xxi     DRAFT-DO NOT QUOTE OR CITE

-------
                 U.S. ENVIRONMENTAL PROTECTION AGENCY
        PROJECT TEAM FOR DEVELOPMENT OF AIR QUALITY CRITERIA
            FOR OZONE AND RELATED PHOTOCHEMICAL OXIDANTS
Scientific Staff

Mr. James A. Raub—Health Scientist, Environmental Criteria and Assessment Office
(MD-52), U.S.  Environmental Protection Agency, Research Triangle Park, NC  27711

Dr. A. Paul Altshuller—Physical Scientist, Environmental Criteria and Assessment Office
(MD-52), U.S.  Environmental Protection Agency, Research Triangle Park, NC  27711

Mr. William G. Ewald—Health Scientist, Environmental Criteria and Assessment Office
(MD-52), U.S.  Environmental Protection Agency, Research Triangle Park, NC  27711

Dr. J.H.B. Garner—Ecologist, Environmental Criteria and Assessment Office (MD-52),
U.S. Environmental Protection Agency, Research Triangle Park, NC  27711

Dr. Judith A. Graham—Associate Director, Environmental Criteria and Assessment Office
(MD-52), U.S.  Environmental Protection Agency, Research Triangle Park, NC  27711

Ms. Ellie R.  Speh—Secretary, Environmental Criteria and Assessment Office (MD-52),
U.S. Environmental Protection Agency, Research Triangle Park, NC 27711

Ms. Beverly  E. Tilton—Physical  Scientist, Environmental Criteria and Assessment Office
(MD-52), U.S.  Environmental Protection Agency, Research Triangle Park, NC  27711
Technical Support Staff

Mr. Douglas B. Fennell—Technical Information Specialist, Environmental Criteria and
Assessment Office (MD-52), U.S. Environmental Protection Agency, Research Triangle Park,
NC 27711

Mr. Allen G. Hoyt—Technical Editor and Graphic Artist, Environmental Criteria and
Assessment Office (MD-52), U.S. Environmental Protection Agency, Research Triangle Park,
NC 27711

Ms. Diane H.  Ray—Technical Information Manager (Public Comments), Environmental
Criteria and Assessment Office (MD-52), U.S. Environmental Protection Agency, Research
Triangle Park, NC  27711

Mr. Richard N. Wilson—Clerk, Environmental Criteria and Assessment Office (MD-52),
U.S. Environmental Protection Agency, Research Triangle Park, NC 27711
December 1993                        H-xxiii     DRAFT-DO NOT QUOTE OR CITE

-------
                 U.S. ENVIRONMENTAL PROTECTION AGENCY
        PROJECT TEAM FOR DEVELOPMENT OF AIR QUALITY CRITERIA
            FOR OZONE AND RELATED PHOTOCHEMICAL OXIDANTS
                                     (cont'd)
Document Production Staff

Ms. Marianne Barrier—Graphic Artist, ManTech Environmental, P.O. Box 12313,
Research Triangle Park, NC 27709

Mr. John R. Barton—Document Production Coordinator, ManTech Environmental
Technology, Inc., P.O. Box 12313, Research Triangle Park, NC  27709

Ms. Lynette D. Cradle—Lead Word Processor, ManTech Environmental Technology, Inc.,
P.O. Box 12313, Research Triangle Park, NC 27709

Ms. Joria R. Followill—Word Processor, ManTech Environmental Technology, Inc.,
P.O. Box 12313, Research Triangle Park, NC 27709

Ms. Wendy B. Lloyd—Word Processor, ManTech Environmental Technology, Inc.,
P.O. Box 12313, Research Triangle Park, NC 27709

Mr. Peter J. Winz—Technical Editor,  Mantech Environmental Technology, Inc.,
P.O. Box 12313, Research Triangle Park, NC 27709
Technical Reference Staff

Mr. John A. Bennett—Bibliographic Editor, ManTech Environmental Technology, Inc.,
P.O. Box 12313, Research Triangle Park, NC 27709

Ms. S. Blythe Hatcher—Bibliographic Editor, Information Organizers, Inc., P.O. Box 14391,
Research Triangle Park, NC 27709

Ms. Susan L. McDonald—Bibliographic Editor, Information Organizers, Inc.,
P.O. Box 14391, Research Triangle Park, NC 27709

Ms. Carol J. Rankin—Bibliographic Editor, Information Organizers, Inc., P.O. Box 14391,
Research Triangle Park, NC 27709

Ms. Deborah L. Staves—Bibliographic Editor, Information Organizers, Inc.,
P.O. Box 14391, Research Triangle Park, NC 27709

Ms. Patricia R. Tierney—Bibliographic Editor, ManTech Environmental Technology, Inc.,
P.O. Box 12313, Research Triangle Park, NC 27709
 December 1993                        U-xxiv    DRAFT-DO NOT QUOTE OR CITE

-------
 i         5.  ENVIRONMENTAL EFFECTS OF  OZONE AND
 2              RELATED PHOTOCHEMICAL OXIDANTS
 3
 4
 5     5.1   INTRODUCTION
 6          Analyses of photochemical oxidants in the ambient air have revealed the presence of a
 7     number of phytotoxic compounds, including O3, peroxyacyl nitrates, and NO2.  Ozone, the
 8     most prevalent photochemical oxidant, has been studied the most and its effects are better
 9     understood than those of other photochemically derived oxidants.  Ozone affects vegetation
10     throughout the United States, impairing crops, native vegetation, and ecosystems more than
11     any other air pollutant (Heck et al., 1980).  The phytotoxicity of nitrogen oxides has been
12     assessed in Air Quality Criteria for Oxides of Nitrogen (U.S. Environmental Protection
13     Agency, 1993) and will not be discussed here.  On the basis of concentration, the peroxyacyl
14     nitrates are more toxic than O3, with PAN being about ten times more phytotoxic than
15     O3 (Darley et al., 1963; Taylor and MacLean,  1970; Pell, 1976).  Although more phytotoxic
16     than O3, the peroxyacyl nitrates generally occur at significantly lower ambient
17     concentrations, however, and phytotoxic concentrations are therefore less widely distributed
18     than those of O3. Ambient concentrations of O3 and PAN, as well as their concentration
19     ratios, are discussed in detail in Chapter 4.
20          The effects of photochemical oxidants were first observed as  foliar injury on vegetation
21     growing in localized areas in Los Angeles County, California (Middleton et al., 1950).
22     In these early reports, foliar injury was described as glazing, silvering, and bronzing of the
23     lower leaf surface of leafy vegetables and as transverse bands of injury on monocotyledonous
24     species.  Subsequent studies showed that these symptoms of photochemical oxidant injury
25     were caused by peroxyacetyl nitrate (Taylor et al., 1960).  The characteristic O3 stipple on
26     grape leaves reported in the late 1950s was the first observation of O3 injury to vegetation in
27     the field (Richards  et al., 1958).  Subsequent studies with tobacco and other crops confirmed
28     that O3 was injuring vegetation at sites near urban centers (Heggestad and Middleton, 1959;
29     Daines et al., 1960).  It is now recognized that vegetation at rural sites may be injured by
30     O3 transported long distances from urban centers (Edinger et al., 1972; Heck et al., 1969;


       December 1993                         5-1       DRAFT-DO NOT QUOTE OR CITE

-------
 1     Heck and Heagle, 1970; Kelleher and Feder, 1978; Miller et al.,  1972; Skelly et al., 1977;
 2     Skelly, 1980; Garner et al., 1989; see also Chapters 3 and 4).
 3           Plant stress from O3 exposures occur when the atmospheric concentrations exceed the
 4     limits of plant tolerance, not because the gas is unique.  Not all plants are sensitive.  The
 5     effects of O3 on terrestrial vegetation begin with the responses of individual plants (see
 6     Figure 5-1).  When there are many sensitive individuals within a population, populations are
 7     affected.  Changes within sensitive populations, or stands, ultimately can affect community
 8     and ecosystem structure and function.  The occurrence and magnitude of the effects depends
 9     on the pollutant  concentration, duration of the exposure, length of time between exposures,
10     genetic composition (i.e., sensitivity) of the plants, and various environmental and biological
11     factors influencing plant response.
12           Foliar injury is usually the first visible sign of O3 exposure and indicates impairment of
13     physiological processes within the leaves. As illustrated in Figure 5-1, in order for O3 to
14     affect an individual plant, sufficient amounts of O3 derived from atmospheric and various
15     canopy processes must be able to reach the leaves of the plant. To  cause injury, ozone must:
16     (1) enter the plant through the leaf stomata; (2) dissolve in the aqueous layer lining the cell
17     walls within the air spaces; and (3) O3 or its decomposition products diffuse through the
18     membrane into the cell, where it can react with cellular components and affect metabolic
19     processes, unless the plant is able to detoxify or metabolize O3 or its metabolites (Tingey and
20     Taylor, 1982).  Cellular injury has been  shown to subsequently manifest itself in a number of
21     ways.  These include: (1) visible foliar injury; (2) premature needle senescence; (3) reduced
22     photosynthesis;  (4) reduced carbohydrate production and allocation; (5) reduced plant vigor;
23     and (6) reduced growth or reproduction or both (McLaughlin et al., 1982; U.S.
24     Environmental Protection Agency, 1986).  The impact of pollutant exposure is determined by
25     the developmental stage, the genetic composition, the complex interactions among natural and
26     pollutant stresses, their temporal and spatial variation, and finally, the action these have on
27     the biochemical and physiological processes within the plants.  Most plants undergo some
28     form of stress during the various stages of their life cycle; however, the multiple stresses
29     they encounter during their lifetimes do not usually all occur at one time (Osmond et al.,
30      1987).
        December 1993                            5-2       DRAFT-DO NOT QUOTE OR CITE

-------
       Atmospheric Processes
         Canopy Processes
           Leaf Processes/
            Ozone Uptake
           Leaf Processes/
           Mode of Action
           Plant Response
        Ecosystem Response
                                            [Reduced Photosynthesis
                                        [Reduced Carbohydrate Production)

                                        '                          '
   [Reduced Carbohydrate Allocation]
                 r
            Compensation
           Reduced Growth ]
                 V
        (Reduced Reproduction)
                  *
        Increased Susceptibility to
        Biotic and Abiotic Stresses
                 T
        Decrease in Mycorrhizae
               Formation
         f Individual Response 1
                  y
         [ Population Response]
                                               [Community Response]
                                               [Ecosystem Response]
Figure 5-1.  Leaf absorption and possible functional changes that may occur within the
           plant. Ecosystem response begins at the level of the individual and is
           propagated upward.
December 1993
5-3
DRAFT-DO NOT QUOTE OR CITE

-------
 1           Ozone can affect all aspects of plant growth (Figure 5-1).  Plants accumulate,  store,
 2     and use carbon compounds to build their structure and maintain physiological processes
 3     (Waring and Schlesinger, 1985).  Within the leaf,  carbon dioxide absorbed from the
 4     atmosphere is converted to carbohydrates during the process of photosynthesis.  The water
 5     and minerals necessary for growth are absorbed by plants from the soil.  Growth and seed
 6     formation depend not only on the rate of photosynthesis and uptake of water and nutrients,
 7     but also on the subsequent metabolic processes and the allocation of the carbohydrates
 8     produced during photosynthesis.  Most plants require  a balance of resources (i.e, energy,
 9     water, and mineral nutrients) to maintain optimal growth, but these are seldom available in
10     natural environments (Chapin et al., 1987).  Plants compensate for injury and/or stresses by
11     allocating their available resources to the point of injury or stress (Mclaughlin et al., 1982;
12     Miller et al., 1982; Tingey et al.,  1976).  Altering the allocation of carbohydrates has been
13     shown to decrease plant vigor, increase susceptibility  to insect pests and fungal pathogens,
14     interfere with mycorrhizal formation and reduce plant growth and reproduction (McLaughlin
15     et al., 1982; Miller et al., 1982; U.S.Environmental Protection Agency, 1986; Garner et al.,
16     1989).
17           Most of our knowledge concerning the effects of O3 on vegetation comes from studies
18     of the responses of important agricultural crop plants  and some selected forest tree species,
19     mostly as seedlings or saplings. Crop plants, because of the importance of their yield to
20     human food demand, usually have been selected for their productivity. In addition, crop
21     plants usually are fertilized, weeded, frequently irrigated and grown in monocultures.
22     In other words, competition for water, nutrients, space and light is greatly diminished when
23     compared to plants growing in natural ecosystems.
24           The number of crop species and cultivars for which information regarding O3  effects
25     exists encompass a mere fraction of the total of those cultivated  as crops or found growing in
26     natural communities.  It is not possible to predict the  sensitivity  of the species and cultivars
27     that have not been  investigated, except in very general terms, because of the wide range of
28     sensitivities to O3 known to exist among the  species that have been studied and even among
29     cultivars of individual crops.  A number of attempts have been made  to develop a general
30     framework of response covering a range of species using the fragmented knowledge
31     available.  All of them have their shortcomings.

       December 1993                            5-4       DRAFT-DO NOT QUOTE OR CITE

-------
 1           Ecosystem responses are hierarchical and range from those that are characteristic of
 2      individual organisms through populations to communities, and ultimately, to ecosystems
 3      (U.S. Environmental Protection Agency,  1978, 1986).  Organisms, not ecosystems, respond
 4      to O3 exposure (Sigal and Suter, 1987).  The only well documented study of ecosystem
 5      change is that of the San Bernardino Forest ecosystem in southern California where the
 6      impact of O3 on the keystone species, ponderosa and Jeffrey pine resulted in the degradation
 7      of the forest (Miller, 1982, 1984; U.S. Environmental Protection Agency, 1978, 1986).
 8      Studies within the forests of the eastern United States, until recently, have dealt with only a
 9      few plant species, chiefly eastern white pine, none of which have been critical in maintaining
10      ecosystem structure and function (McLaughlin et al., 1982; Skelly, 1980; Skelly et al., 1984;
11      U.S. Environmental Protection Agency,  1978,  1986).  The absence of long term studies
12      dealing with the impacts of O3  on various ecosystem components and how these influence
13      ecosystem structure and functions makes determination of the impact of O3 on ecosystems in
14      general difficult.
15           The sequential organization of this  chapter closely follows the discussion dealing with
16      the responses of plants  to O3 presented above.  First, the methodologies (Section 5.2) that
17      have been used to obtain the information on which the rest of the chapter is based are
18      described.  The next section (5.3) details the known  biochemical and physiological responses
19      occurring within leaf cells after O3 entry into the leaves and how these responses affect plant
20      vigor, growth,  productivity and reproduction.  Factors within and external to plants influence
21      their response to O3 and other stresses.   How  these factors, observed during experimentation
22      or in the field,  can modify functional and growth responses of plants exposed to O3 is
23      presented in the next section (Section 5.4).
24           A complicating factor in assessing plant response to O3 exposure is determining the
25      amount of O3 entering the leaves. Entry of O3 into  plant leaves is not a simple uptake
26      process, but involves gas exchange; the entry of O3 through the stomata and carbon dioxide
27      (CO2) from the atmosphere at the same time oxygen and water vapor are exiting. For many
28      years, attempts have been made to develop mathematical equations that quantify the
29      relationship between pollutant exposure and agricultural crop yield.  The problem is the need
30      for combined incorporation of the age and the genetic composition of the plant, along with
31      parameters for pollutant concentration, duration, frequency of exposure and the respite  time

        December 1993                           5,5        DRAFT-DO NOT QUOTE OR CITE

-------
 1     between exposures into an exposure statistic or index which may be used to predict crop
 2     yield loss.  Section 5.5 discusses the strong points and shortcoming of the various indices
 3     that  have been developed to aid in predicting the effects of O3 on crops.
 4          Some O3 exposures (concentration and duration) result in foliar injury to the plant.
 5     Other exposures result in growth reduction and decrease in productivity. Section 5.6,
 6     exposure-response of plant species, presents the data from many different experiments and
 7     assesses the potential impact of different concentrations and exposure durations on growth of
 8     a variety of plants ranging from cultivated annual crops to woody perennials such as trees
 9     and shrubs.  Of particular interest is the yield of crops.  The  majority of the data concerning
10     the response of ecosystems deals with the response of individual organisms, populations or
11     forest stands.  Therefore, in section (5.7)  the knowledge concerning ecosystem response to
12     perturbations obtained from a variety of studies, and the California San Bernardino Forest
13     study in particular, is used to present a view  of what might be expected from continued
14     O3 exposure.
15          The costs to the nation of O3 exposure of crops and ecosystems is discussed in
16     Section 5.8.  The scientific names of the plants cited in this chapter are presented in a table
17     in Appendix A.  Section 5.9 discusses the effects of O3 on nonbiological materials, followed
18     by an integrative summary and conclusions section (5.10) drawing together and interpreting
19     key information from the earlier chapter sections concerning vegetation effects.
20
21
22     5.2    METHODOLOGIES USED  IN VEGETATION RESEARCH
23     5.2.1   Fumigation Systems
24          The methodologies used in vegetation research have become more sophisticated over
25     the years as new technology has developed.  New exposure systems have been devised with
26     pollutant dispensing systems that make it  possible to more nearly duplicate the exposures
27     plants receive in the field. These systems and their good points and short-comings are
28     discussed below.
29           Air pollution exposure-response studies usually require exposure chambers or other
30     apparatus for maintaining controlled pollutant exposures.  Ozone exposure systems are
31     designed to maintain a modified gaseous atmosphere around a plant for a period of exposure,

       December  1993                           5-6       DRAFT-DO NOT QUOTE OR CITE

-------
 1      for the purpose of monitoring plant responses to that modified gaseous atmosphere.
 2      Whichever system is used, they all share some features in common, namely:  general plant
 3      growth conditions (light, temperature, humidity, carbon dioxide, soil water) must be met,
 4      and differential concentrations  of O3 generated either artificially or naturally must be
 5      supplied to the fumigation system.  Exposure systems have been established in controlled
 6      environments, greenhouses and the field, many of these were described in the earlier criteria
 7      document, Air Quality Criteria for Ozone and Other Photochemical Oxidants (U.S.
 8      Environmental Protection Agency,  1986).  Exposure systems may range from cuvettes which
 9      enclose leaves or branches (Bingham and Coyne, 1977; Legge et al.,  1979) to a series of
10     tubes with calibrated orifices spatially distributed over a field to emit gaseous pollutants to a
11      plant canopy (Lee et al.,  1978). Each type of system was designed for specific objectives
12     and operates most efficiently under the conditions for which it was intended.  Each  has
13     advantages and limitations and must be evaluated in terms of the objectives it was designed
14     to meet.
15
16     5.2.1.1   Methodologies Discussed in the Air Quality Criteria for Ozone and Other
17               Photochemical Oxidants (1986)
18     Controlled Environment Exposure Systems
19           Controlled environment fumigation systems are those in which light sources, and
20     control of temperature and relative humidity are artificial. Light quality  and quantity  are
21     likely to be lower than in ambient environments, usually resulting in lower photosynthetically
22     active radiation (PAR). Temperature and relative humidity will likely be more consistent in
23     a controlled environment than in ambient air.  Controlled environment exposure systems are
24     typified by the widely-used continuous stirred tank reactor (CSTR), a system originally
25     designed for mass balance studies of O3 flux to vegetation.  The main benefit of controlled
26     environment chambers is that the environmental conditions during exposure can be very well
27     characterized, controlled and replicated over time.  They  work very well for evaluating
28     O3 effects on physiological processes, which are themselves sensitive to changes in  other
29     environmental parameters.  The major limitation of controlled environment exposure systems
30     is the extrapolation  of the data to field situations.
31           Greenhouse system designs are similar to those found in controlled  environments,
32     except that light, temperature and relative humidity conditions fluctuate with those occurring
       December 1993                            5-7       DRAFT-DO NOT QUOTE OR CITE

-------
 1     in the greenhouse. Thus, they are more closely related to field studies than are controlled
 2     environments, but plant culture and environmental conditions are still quite different from
 3     those of field exposure chambers, making direct extrapolation difficult.  These studies are,
 4     however, more applicable to phytotoxicity of O3 to greenhouse grown ornamental and
 5     floriculture crops (U.S. Environmental Protection Agency, 1986).  Some greenhouse
 6     exposure systems use activated charcoal filtration to remove pollutants from the incoming air
 7     prior to the addition of experimental O3, and either vent directly to the outside, or use
 8     charcoal filtration of the outgoing air to prevent contamination of the greenhouse air supply.
 9     Other greenhouse exposure  systems filter neither incoming nor outgoing air.
10
11     Field Exposure Systems
12          Fumigation of plants with O3 in the field is most frequently carried out using open-top
13     chambers.  The most widely utilized design (U.S. Environmental Protection Agency, 1986)
14     consists of a cylindrical aluminum frame, covered with transparent film. The bottom half of
15     the transparent covering is doubled layered, the inside panel  of which is perforated.
16     Charcoal and particulate filtered air, non-filtered air or O3 supplemented air is blown into the
17     bottom  layer, forced through the perforations into the plant canopy, and then escapes through
18     the top  of the chamber.  The positive pressure maintained by the forced movement of air up
19     through the chamber minimizes influx of ambient air into the chamber through the open-top.
20     The open-top chamber exposure system was employed in the National Crop Loss Assessment
21     Network (NCLAN) from 1980 to 1988 and a description and discussion of the chambers is
22     provided in the 1986 criteria document Section 6.2.4  (U.S. Environmental Protection
23     Agency, 1986).  The design of these chambers has been modified with frusta to reduce such
24     incursions by ambient air, making the chambers more viable under windy conditions.
25     Canopies (moveable) have been added so that rain exclusion  studies can be carried out.
26     Finally, they have been modified in  shape or increased in size so that species such as mature
27     trees and grapevines can be enclosed.  Crop loss studies conducted in open-top chambers
28     more closely simulate field  losses of crops due to O3  than controlled environments or
29     greenhouse fumigation chambers. However, there are some important differences in
30     environmental conditions between open-top chambers and the field.  Specifically, the frusta
31     and walls of the chamber block some incoming light, as well as trap some long-wave

       December 1993                           5-8       DRAFT-DO NOT QUOTE OR CITE

-------
  1      radiation within the chamber, so that PAR levels are lower and temperatures are higher in
  2      the chambers than in the field.  The walls also cause a rain shadow necessitating irrigation.
  3      The rate at which air moves across the foliage contributes significantly to canopy resistance
  4      to O3 uptake,  and  is similar between chambered and non-chambered plants.  This suggests
  5      that O3 uptake by the foliage is similar between open-top chambers and the field (U.S.
  6      Environmental Protection Agency, 1987).  To promote normal dew formation, many studies
  7      turn off the blower fans during the night.
  8           Limited use (for O3 studies) has been  made of chamberless field exposure systems,
  9      which rely on ambient wind conditions to move O3 across an open field canopy. The O3 is
10      emitted from vertical pipes, which are spaced in a circle around the experimental plot of
11      plants.  The amount of O3  emitted from each vertical pipe, as well  as the number and
12      compass direction  of emitting pipes, depends on the wind direction  and speed, this whole
13      process usually being computer controlled.
14
15      5.2.1.2   Methodologies Referenced Since the Air Quality Criteria for Ozone and Other
16               Photochemical Oxidants (1986)
17      Branch and Leaf Chambers
18           Most of the developments in exposure systems since 1986 have been modifications of
19      existing systems. The  tremendous interest in evaluation of mature tree response to O3 has
20      prompted the development  of large branch chambers for estimating  O^ flux to trees.  These
21      branch chambers share many of the design characteristics of a CSTR.  The chamber walls
22      are transparent film spread over a supporting frame, there is a fan to reduce boundary layer
23      resistance across the foliar  surface, and an air inlet and outlet so that differential O3, carbon
24      dioxide (photosynthesis) and water vapor (leaf diffusive resistance) measurements can be
25      taken (Ennis et al., 1990; Houpis et al., 1991; Teskey et al., 1991). The advantages of this
26      system include the ease with which the Teflon bag can be replaced, uniform light
27      transmission can be maintained, the branch  chamber can be moved from plant-to-plant, can
28      be used in situ, and can be modified for different sized branches.  One of the disadvantages
29      of the branch chamber, and indeed of any such cuvette which isolates one part of the plant
30      under different environmental conditions than the rest of the plant, is whether the isolation
31      leads to a response different from that which would have been observed if the branch was
32      under the same environmental conditions as the rest of the plant.  In addition, total tree
        December 1993                           5.9       DRAFT-DO NOT QUOTE OR CITE

-------
 1     growth cannot be estimated using branch chambers, as only part of the plant is treated with
 2     O3.
 3
 4     5.2.1.3   Flux Measurement
 5          Estimation of O3 flux to foliage can be made directly, by measuring the difference in
 6     O3 concentration between air going into a leaf chamber and the same air stream  exiting the
 7     chamber after passing over the leaf. It can also be inferred from measurements  of leaf
 8     diffusive resistance during exposure of a leaf to O3. The former method requires a chamber
 9     or cuvette fumigation system with uptake of O3  which is quite small or extremely
10     nonvariable relative to the amount being taken up by the leaf.  Otherwise, it is difficult to
11     detect O3 flux to a leaf with good precision.  Such  cuvettes can be adapted from those
12     commercially available for portable photosynthesis meters (Graham and Ormrod, 1989) or
13     constructed from a novel design, such as that developed by Fuentes and Gillespie (1992) to
14     estimate the effect of leaf surface wetness on O3 uptake of maple leaves.  The criteria for
15     flux cuvette design include  good light  transmissibility, ease of leaf manipulation, minimal
16     reaction  of chamber  wall surface with O3 and good air mixing within the chamber.  Good
17     mixing of air is necessary to avoid a gradient in pollutant concentration, and to maintain a
18     boundary layer resistance which is greater than  stomatal resistance.  Maintenance of leaf
19     temperature close to that of the surrounding air, so that transpiration rates are not abnormally
20     high, is another benefit of good air mixing.  The physical design of the Fuentes  and Gillespie
21     chamber was simple, consisting of two glass hemispheres that were clamped together,
22     separated by a Viton O-ring, over the petiole of the leaf under investigation. Inlet and outlet
23     air attachments were on opposite sides of the cuvette.  Other cuvette designs have been used
24     to estimate leaf gas exchange responses to O3; their principals of operation are similar, but
25     there are differences in materials and  design (Amiro et al., 1984; Freer-Smith and Dobson,
26     1989; Laisk et al., 1989; Moladau et al., 1991; Skarby et al.,  1987).
27           Compared to the CSTR, which has been used for mass balance measurement of gas flux
28     by whole plants during fumigation (LeSueur-Brymer and Ormrod, 1984), cuvette systems
29     usually determine flux to one leaf at a time.  This results in a more precise understanding of
30     the interaction among leaf age, leaf diffusive resistance, leaf illumination and  O3 flux.
31     However, these data are not particularly well adapted to estimating flux of O3 to a  large

       December 1993                           5-10      DRAFT-DO NOT QUOTE OR  CITE

-------
  1      vegetated surface.  Finally, regardless of the methodology used to determine O3 flux to
  2      foliage, there exist only very sketchy mechanistic-process models which would link O3 fluxes
  3      to decreases in growth and productivity of plants.  At this time, these data are mainly useful
  4      for developing a relationship between internal O3 dose and plant response, and estimating the
  5      strength of vegetation as sinks for O3 flux  on a large scale.
  6
  7      Pollutant Dispensing Systems
  8           Although exposure chambers have changed little in design in the last several years, the
  9      profile characteristics and method of dispensing pollutant profiles have.  Whereas early
10      studies utilized static or square-wave exposures, usually controlled by hand-set flowmeters,
11      many more recent system expose plants with so-called dynamic exposures, during which the
12      O3 concentration gradually reaches  a maximum, thus simulating diurnal variation in
13      O3 concentration (Hogsett et al., 1985a).  These profiles may be achieved by mass flow
14      controllers that are themselves computer controlled.  Proportional add systems such as that
15      used in NCLAN usually achieve ambient type profiles using rotameters instead of mass flow
16      controllers.  The O3 concentration in each  of the chambers is logged at pre-set intervals, so
17      that the integrated exposure for  the entire fumigation period can be calculated.  Deviations
18      from the planned O3  episode can occur, due  to failure in dispensing or monitoring
19      equipment, as well as incursions of air through the tops of the chambers.  The length of the
20      interval between determinations  of O3  concentration in the chambers can be  an important
21      contribution to the control of O3 profile. In  general, longer intervals lead to less well-
22      controlled  and well-characterized O3 exposure profiles (Lefohn et al., 1993). These
23      deviations  from the expected profiles can be  mathematically quantified, and monitored among
24      treatments  and replications (Hale-Marie et al., 1991).
25
26      Open Air Field Fumigation Systems
27           Open air field fumigation systems have the potential to most closely estimate filed
28      losses due  to O3, as the plants are grown and exposed under ambient field environmental
29      conditions.  However, of all the fumigation systems, this is the least controllable and
30      repeatable.  It has been used in the past to  expose plants  to "static" concentrations (desired
31      concentration is the same throughout the exposure period) of such pollutants as sulphur

        December  1993                           5. j j       DRAFT-DO NOT QUOTE OR CITE

-------
 1     dioxide or hydrogen fluoride (Hogsett et al., 1987). The Zonal Air Pollution System (ZAPS)
 2     has been vastly modified and improved upon to enable fumigation of plants with the diurnally
 3     varying pattern of concentration typical of ambient O3 fumigation (Runeckles et al., 1991).
 4     The system represents a significant advancement over earlier open-air field fumigation
 5     systems, in, that 12 discrete seasonal treatments which simulate ambient patterns are achieved
 6     rather than the usual two or three. Ozone was supplied to plots, which were laid out in
 7     groups of four, through a manifold suspended  over the plant canopy. The wind speed and
 8     direction determined the actual seasonal O3 exposures, although the O3 was released in
 9     concentrations proportional to that observed at the time in the ambient environment.  While
10     the twelve treatments are not repeatable over time, a regression relationship between
11     pollutant exposure and plant response can be established for each growing season.
12           The Liphook study in England of long-term responses of Picea sitchensis (Bong.) Carr,
13     Picea abies  (L.) Karst., and Pinus sylvestris L. to sulphur dioxide and O3 in combination
14     consisted of seven growth plots, 50 m in diameter, five of which were surrounded by
15     64 vertical pipes from which pollutant gasses were emitted  (McLeod et al., 1992).  The
16     64 pipes were divided into four quadrants  of 16 adjacent  pipes, and each quadrant had diluted
17     pollutant gases supplied to it from a computer controlled  mass flow controller. The emitting
18     quadrant(s) as well as the rate at  which the gases were supplied to the quadrant depended on
19     wind speed and direction.  The gases were emitted from  the vertical pipes into the  plant
20     canopy at two heights, 0.5 and 2.5 m above a reference height, which was approximately
21     two-thirds of tree  height.  This pattern of gas dispersion  resulted in a uniform horizontal
22     distribution  of hourly mean gas concentration across each central 25-m diameter experimental
23     plot. Measured over a  winter wheat canopy, SO2 concentration differed by less than 1 nl.l"
24     over a 5-h period  of measurement; measurement of consecutive 2-min mean values at five
25     locations across the plots demonstrated high uniformity (McLeod et al., 1985).  This
26     exposure system,  like all open-air exposure systems, clearly simulates field plant growth
27     conditions far better than open- or closed-top chambers.  The usefulness of the data is limited
28     however, by the low number of treatments and lack of replication of those treatments.  And,
29     with five "enclosures",  and two nonenclosed ambient plots, this is by far the largest of the
30      very few of these systems which are  in operation.
31

        December 1993                           5-12       DRAFT-DO NOT QUOTE OR CITE

-------
  1      Field Chamber Exposure Systems
  2           Open-top field chambers are used in most field studies of plant response to gaseous
  3      pollutants.  They were first designed for studies on annual herbaceous crop plants (Mandl
  4      et al., 1973) but enlarged versions have been used successfully in tree seedling and sapling
  5      studies also (Adams et al., 1990; Chappelka et al., 1990; Qui et al., 1992; Kress et al.,
  6      1992; Hogsett et al., 1989;  Andersen et al., 1990; Karnosky et al.,  1993; Wang et al., 1991;
  7      Temple et al.,  1991).  Because the results from these studies using tree species are
  8      extrapolated to predict the effects of O3 on forests, these studies require good exposure
  9      control in order to  replicate ambient O3 profiles characteristic of many low-elevation, rural
 10      areas of eastern North America.  This condition could have been met using an open field
 11      exposure system.  Open-top chambers which are large enough for mature trees to  have been
 12      developed but are expensive (Grandl et al.,  1989).
 13           Microclimatic modification by open-top chambers as well as O3 exposure schedules
 14      which are disconnected from typical  O3 episode meteorology have been addressed in a
 15      seasonal study of tree response to O3 in the United Kingdom (Wiltshire et al., 1992). This
 16      study is using open top chambers with roll-up sides;  except for fumigation days, the plants
 17      are maintained in ambient climatic conditions.  The exposure episodes number between
 18      27 and 30 throughout the growing season, and occur on days with ambient meteorology
 19      associated with naturally occurring O3 episodes (i.e., high incident radiation and temperature
 20      with little air movement) (Wiltshire et al., 1992).  The maintenance of near-ambient
 21      meteorological  conditions during both growth and exposure periods ensures that this study
 22      will represent field  grown plant responses to O3 better than traditional open-top chamber
 23      studies.
 24           Several designs of field fumigation chambers have been developed to overcome some of
 25      the disadvantages of the open-top chambers, namely small plot size and incursion of ambient
 26      air.  Closed top chambers were first  developed in the 1950's; generally,  smaller in dimension
 27      to the open-top design, have been more recently constructed in California to assess crop loss
28      to O3.  Closed  top chambers were chosen because the authors wished to characterize the
29      pollutant dose to the plants very precisely; pollutant gradients within the  chamber were
30      minimal (Musselman et al.,  1986). The chambers were octagonal in shape and covered with
31      Teflon® film; the soil was completely replaced with standard greenhouse mix. Temperatures

        December 1993                            5_13       DRAFT-DO NOT QUOTE OR CITE

-------
 1     in the chamber were higher (2 to 4 °C at midday,  1 to 2 °C at night) than in the ambient air,
 2     and light levels were reduced by  11 % (spectral quality of the light in the chambers was not
 3     reported).  The authors concluded that, although the chambers were not suitable for studies
 4     requiring close approximation of field conditions, they were very useful when tight control
 5     over soil moisture and pollutant concentration were needed.
 6          Closed-top chambers  were  constructed and installed in the United Kingdom to study
 7     responses of shrubs and large herbaceous species to long term, low  (chronic) concentrations
 8     of sulphur dioxide, nitrogen dioxide and O3 (Rafarel and Ashenden, 1991).  They were a
 9     smaller version of an earlier design, as the larger chambers required pure gas sources of
10     nitrogen dioxide and sulphur dioxide to be  diluted  into the ventilating air stream, which
11     resulted in highly variable exposure concentrations. The flow rate of the smaller chambers
12     meant that premixed gases  were sufficient to maintain steady control of treatment
13     concentrations.  Because the gases were discharged from the source at constant
14     concentrations, different treatments were achieved  by  placing one or more pollutant supply
15     tubes in the fumigation chambers. Good air circulation (and moderate ambient temperatures)
16     maintained the domes at near ambient conditions.
17
18     Ambient Gradients for Evaluation of Plant Response to Ozone
19          The exposure system  which most simulates ambient conditions of O3 exposure,
20     temperature, humidity, soils, soil moisture, is  the ambient gradient system.  By this method,
21     plants are  grown along a transect of known differential pollutant concentrations, usually
22     downwind of a major point source or urban area.  The concentration of pollutant(s) is diluted
23     as distance from the source increases.  A study of four cultivars of red clover (Trifolium
24     repens  L)  and spring barley (Hordeum vulgare L)  was conducted along such a transect of
25     gradient sulphur dioxide, nitrogen dioxide, and O3 concentrations in the United Kingdom
26     (Ashmore et al., 1988).  Ozone concentration  was inferred from injury to Bel W3 and Bel B
27     cultivars of tobacco, but was found to have very little relationship to cultivar performance.
28     The authors  cautioned that these results must be interpreted with an understanding that
29     differences among sites in  other environmental parameters could contribute to the detection
30      (or failure to detect) of O-j effects on the crops. For ambient gradient  studies to be
31      interpretable, good characteri/.ation of site parameters (rainfall, temperature, radiation, soil

        December 1993                           5-14       DRAFT-DO NOT QUOTE OR CITE

-------
 1     type) is needed. Additionally, the modeler needs to know how these factors should be used
 2     to adjust the apparent plant response.  In order to know that, a good knowledge base of how
 3     all of these factors modify plant response to O3 is needed.
 4          At this time, although some information is available, the relationships are still
 5     incompletely understood.  Many investigators consider that ambient gradients are impossible
 6     to find without major differences in environmental conditions which may affect plant
 7     response to  O3 and therefore confound interpretation of the results.
 8
 9     Comparison of Fumigation Systems
10          Each type of fumigation system is particularly well suited to certain types of studies of
11     plant response to O3.  To gather data relevant to the mechanisms of plant response to O3,
12     chambers with a high degree of control over environmental conditions are  needed.  Many of
13     the physiological bases of plant response to O3 can be themselves  highly influenced by small
14     differences in light, humidity, and temperature.  For example, measurements of O3 effects on
15     photosynthetic rates in chambers with illumination levels well below saturation for
16     photosynthesis may be highly variable with very small changes in  PAR, as the relationship
17     between PAR and photosynthetic rates  for many species is steeply linear at low light levels.
18     Alternately, it is notoriously  difficult to get reliable photosynthetic data from field chambers
19     under ambient light, as cloud cover and diurnal changes in the solar angle  cause change in
20     instantaneous  rates of photosynthesis.   For high precision in estimating photosynthetic
21     responses to O3, controlled environment exposure chambers with saturating light sources are
22     needed; such systems are not yet in wide-spread use.
23          A comparison of plant growth and plant  response to O3 fumigation in open-top
24     chambers, closed-top chambers, and air exclusion systems has been carried out (Olszyk
25     et al., 1986).  The authors discovered that there was interaction between plant response to
26     O3 and type of exposure system for less than 10% of the growth parameters measured in
27     California, suggesting  that plant response to O3 was the same regardless of fumigation
28     system.  Plants from exclusion systems were shorter than in open-top chambers, and
29     generally weighed more.  Of the three  groups  of plants, those in the control plots of the
30     exclusion system (i.e., receiving ambient O3 exposure) were most similar in size to plants
31     grown in field plots.  While this and another study (Olszyk et al.,  1992) indicate that

       December 1993                           5_15      DRAFT-DO NOT QUOTE  OR CITE

-------
 1     environmental modification caused by chambers will affect plant growth, there is no evidence
 2     that there is a large effect of chambers on plant response to 63.  It is assumed that, because
 3     of the decreasing relative effects on plant environment caused by controlled environment,
 4     greenhouse, closed cop field chambers, open-top field chambers, open air systems, and
 5     ambient gradients, the system effects on  plant response to O3 will decrease in the same
 6     order.
 7          Considerable concern  has been raised about plant response to trace pollutants in
 8     exposure chambers, specifically N2O5 and NO in chambers receiving O3 generated from dry
 9     air, and NO2 in chambers receiving  ambient air.  These trace pollutants may have a direct
10     effect (positive or negative) on plant processes, or may change how plants respond to O3,
11     and without careful evaluation, these effects may go undistinguished from those of O3.
12     A comparison of alfalfa response to  the same O3 exposure, generated electrostatically from
13     air or through nonfiltration of ambient air, indicated that the generated O3 treatment was
14     more phytotoxic than the ambient Q3 treatment, likely due to the co-generation of N2O5 and
15     NO along with O3 from dry air (Olszyk  et al., 1990).  The results of this study and the
16     comparison among field exposure systems, suggest that estimates of plant response to
17     O3 from open field air exclusion systems will be most representative of true field response,
18     as this system uses ambient O3 and no chambers.  Next in accuracy will be open-top
19     chamber studies using filtered versus nonfiltered ambient O3.  The drawback of these two
20     approaches  is that plant responses to low ambient levels of O3 as might occur in many  years
21     is quite subtle. To detect statistically significant differences between filtered and nonfiltered
22     chamber grown plants requires a high number of replications (Rawlings et al., 1988).   Since
23     seasonal O3 concentrations vary greatly with geographic location and year, the collection of
24     data for yield loss estimates by either of these two methods will be much slower than if
25     O3-enriched chamber exposure systems are used.
26
27     5.2.2   Experimental Design and Data Analysis
28          The statistical design  of an experiment is crucial in defining the types of analyses to
29     which the data can be subjected, and consequently the kinds of information about plant
30     response to O3.  For these reasons,  the information goals of a study must be clearly defined
31     in order to  choose an appropriate experimental design. The various experimental designs and

       December 1993                           5-16      DRAFT-DO NOT QUOTE OR CITE

-------
  1      approaches to data analysis have been well reviewed in the 1986 criteria document (U.S.
  2      Environmental Protection Agency,  1986) and will not be repeated here.  In summary, it is
  3      clear that over the last 15 years, studies have more  frequently used experimental designs
  4      which generate data suitable for determination of regression-type dose-response relationships.
  5      These exposure-response relationships generalize the mathematical relationship between the
  6      plant parameter of interest and O3 exposure.  Plant  response to concentrations other than
  7      those used in the experiment can be interpolated from these relationships and thresholds  of
  8      plant response can be determined (Ormrod et al., 1988).  In the latter half of the NCLAN
  9      program, the Weibull model was chosen to characterize yield response to O3 because of its
 10      flexibility to describe a wide range of data patterns  (Rawlings and Cure, 1985) and,
 11      consequently to allow a common model to be fit when pooling data across years and sites
 12      (Lesser etal., 1990).
 13           Experimental designs for exposure-response relationships can easily be expanded so that
 14      plant response to O3 and another factor at multiple levels can be determined. Because of the
 15      need to contain each O3 treatment by a chamber, incomplete factorial designs are a more
 16      efficient approach to multi-factor studies,  leading to exposure-response surfaces (Allen et al.,
 17      1987).  Choosing the appropriate incomplete factorial design for a response surface study
 18      requires forethought on whether all areas of the surface are of equal interest. For many
 19      O3 plant response studies this is not so, as extremely high concentrations, although increasing
 20      the precision with which plant response to lower concentrations is estimated, are not as likely
 21      to occur in the ambient environment.
 22           Because the U.S. Environmental Protection Agency (1986) decided to place greater
 23      emphasis on damage (i.e., effects that reduce the intended human use of the plant) than on
 24      injury, studies have more frequently used experimental designs which generate data suitable
25      for regression and treatment mean separation analyses to model and test the impact of O3 on
 26      plant response.  While the impact at current O3 levels is of primary interest and can be
 27      studied using two O3 levels generated by charcoal-filtered (CF) and nonfiltered (NF)
 28      treatments, the development of exposure-response models necessitates the use of additional
29      treatments  at above ambient concentrations.  The optimal number, range, and spacing of
30      treatment levels depends upon the anticipated exposure-response model but, in the case of the
31      Weibull and polynomial models, greater precision for estimation of relative yield loss at

        December  1993                           5_17      DRAFT-DO NOT QUOTE OR CITE

-------
 1     ambient O3 concentration is obtained when the lowest treatment level is near zero and the
 2     highest treatment level is well above ambient.  For the Weibull model, the highest treatment
 3     should correspond to a concentration where yield loss is at least 63% of the yield at zero
 4     exposure (Basset and Rawlings,  1988; Rawlings et al.,  1988).
 5          When studying the impact of mixtures of pollutants on plant processes in chambers,
 6     response surfaces can be generated from complete or incomplete factorial designs. These
 7     designs have been shown to increase the precision and efficiency of estimating relative yield
 8     loss at ambient concentrations. (Allen et al., 1987). The optimal design cannot be specified
 9     a priori and necessitates the use of treatment levels from near zero to well above ambient for
10     each pollutant. However, response surface designs have not been widely used in pollutant
11     mixture studies to date. Nor have these designs been widely used to study the interaction
12     between pollutant exposure and quantitative environmental parameters such as light,
13     temperature or soil moisture. The interaction between O3  and phytotoxic concentrations of
14     other pollutants, in particular sulfur dioxide, has not  been extensively studied because
15     instances of co-occurrence of O3 and other pollutants are not common in the United States.
16     An analysis of pollution monitoring data showed fewer than 10 periods  of co-occurrence
17     between O3 and phytotoxie concentrations of sulfur dioxide during the growing season at the
18     sites where the two pollutants were monitored (Lefohn and Tingey, 1984; U.S.
19     Environmental Protection  Agency, 1986).
20           Design and analysis  of pollutant effects studies  have used various  characterizations of
21     exposure to determine optimum spacings of treatment levels and to relate exposure to
22     response.  Most notably, the daytime mean concentration index (i.e., either M7 or M12) has
23     been adopted by the NCLAN program to determine the effects of O3 on plant response.
24     However,  there has been considerable debate over the use of the mean  index in
25     exposure-response modelling; the variety of ways to  compute the characterizations of plant
26     exposure will be discussed elsewhere in this document  (Section 5.5). When plant yield is
27     considered, plant response is affected by the concentration of exposure as well as by other
28      exposure-dynamic factors (e.g., duration,  frequency, threshold, respite time) in combination
29      with physiological, biochemical, and environmental factors which may  mask treatment effects
30      over the growing period.  Research goals to understand the importance of exposure dynamic
31      factors have utilized experimental designs that apply two or more different patterns of

        December 1993                           5-18       DRAFT-DO NOT QUOTE OR CITE

-------
 1      exposure that are equal on some scaling (e.g., total exposure).  Experiments designed
 2      specifically to address the importance of components of exposure may require the use of
 3      exposure regimes that are not typical of the ambient environment.
 4          In experiments in which treatments are quantitative, the traditional approach is to use
 5      regression  analysis which relates O3 exposure to plant  response (U.S. Environmental
 6      Protection  Agency, 1986).  The regression approach has been used to fit a common model to
 7      combined data from  replicate studies of the same species when it is reasonable to assume that
 8      the primary cause of biological response is pollutant exposure and that differences in
 9      environmental, edaphic, and/or agronomic conditions among sites do not significantly change
10      the shape of the regression relationships.  When pooling data across sites and years,
11      additional terms for  site and year effects are often included in the model as either fixed or
12      random components, depending upon the population of interest.  Inferences over random
13      environments implies that the environments sampled by the experiments are representative of
14      the population of regions of interest under a variety of environmental conditions.  In this
15      case, site and year effects are incorporated as random components in the model when fitting
16      a common  model. The appropriate analysis  is to use a mixed model analysis to fit an
17      exposure response model with variance components. This analysis has been recently used to
18      combine data from replicate studies of varying durations to test the importance of length of
19      exposure in influencing plant response;  this approach is described elsewhere in the document
20      (Section 5.5).
21
22      5.2.3   Mechanistic Process Models
23          In addition to regression type models of plant response to O3, which are empirical and
24      statistical in nature, there are mechanistic-process models (Luxmoore, 1988; Kickert and
25      Krupa, 1991; Weinstein et al., 1991). The key difference between these two types of models
26      is how the  changes in the dependent variable over time are handled.  Empirical models treat
27      a time period (e.g., a growing season) as a single point, and report the response of the
28      dependent variable as a single point as well.  Regression models may also over-simplify the
29      characteristics of an  O3 exposure, in that the description of the O3 exposure is compressed
30      over time to a single number.  The variety of ways to compute this single number will be
31      discussed elsewhere in this document (Section 5.5).

        December  1993                           5_ \ 9      DRAFT-DO NOT QUOTE OR CITE

-------
 1          Mechanistic-process models on the other hand describe the rate of change of a variable
 2     in response to the treatment (such as O3) with change in time (dy/dt).  The latter type of
 3     model has the potential to capture the interaction among plant age/stage of development,
 4     variability of ambient exposure concentrations and plant response to Oj.  For this reason,
 5     mechanistic-process models have been rated much more highly than regression models for
 6     their realism, scientific value and applicability to other locations (Kickert and Krupa, 1991).
 7     However, compared to regression models, mechanistic-process models require more input
 8     data and the input data are less accessible. The mechanistic-process models are more
 9     complex than regression models, requiring more computer time and memory to develop.
10     The precision of the output regression models is greater than mechanistic-process models (for
11     interpolative examinations only), as is their ability to estimate response probabilities.  The
12     authors conclude that the popularity of single-equation time-lumped models is related to the
13     fact that the studies of plant responses to O3  are more oriented to air quality standard setting
14     as an endpoint, rather than the physiological  processes underlying plant responses. The
15     problems with process-based models are the  necessity for some large assumptions (in place of
16     real data) and the lack of validation.  Without that validation, using estimates from these
17     models is questionable.  If these estimations  are used, the uncertainties associated with them
18     must be identified and quantified.
19
20
21     5.3   SPECIES  RESPONSE/MODE  OF ACTION
22     5.3.1   Introduction
23           Plant adaptation to  changing environmental factors or to stresses  involves both short-
24     term  physiological responses and long-term physiological, structural, and morphological
25     modifications.  These changes help plants to minimize  stress and maximize the use of
26     internal and external resources.  A great deal of information is available on the physiology of
27     single leaves, however, relatively little is known about whole-plant systems and whether the
28     physiological mechanisms involved are initiated wholly within the leaf or are the result of
29     whole-plant interactions (Dickson and Isebrands, 1991).
30           The many regulatory systems contained in leaves change both as a function of leaf
31      development and in response to different environmental stresses.  Leaves function as the

        December 1993                           5-20      DRAFT-DO NOT QUOTE OR CITE

-------
 1     major regulators of anatomical and morphological development of the shoot and control the
 2     allocation of carbohydrates to the whole plant (Dickson and Isebrands, 1991).  This section
 3     discusses the movement of O3 into plant leaves and what is known about their biochemical
 4     and physiological responses.
 5           Movement of O3 into plant leaves involves both a gas and a liquid phase.  The
 6     phytotoxic effects of air pollution on plants appear only when sufficient concentrations of the
 7     gas diffuse into the leaf interior  and pass into the liquid phase  within the cells.  Therefore, to
 8     modify or degrade cellular function O3 must  diffuse in the gas-phase from the atmosphere
 9     surrounding the leaves through the stomata into the air spaces and enter into the cells after
10     becoming dissolved in the water coating the cell walls (U.S. Environmental Protection
11     Agency, 1986).  The exact site or sites of action are not known. Biochemical pathways are
12     closely interrelated, and at the present time, we do not have sufficient knowledge of all the
13     control and regulatory mechanisms (Heath  1987).  The previous criteria document
14     summarized quite well the overall  processes controlling plant response to O3:
15             "The response of vascular plants to O3 may  be viewed as the culmination of a
16             sequence of physical,  biochemical, and physiological events.  Ozone in the
17             ambient air does not impair processes or performance, only the O3 that
18             diffuses into the plant. An effect will occur only if a sufficient amount of
19             O3 reaches the sensitive cellular sites  within the leaf. The O3 diffuses from
20             the ambient air into the leaf through the stomata, which can exert some control
21             on O3 uptake to the active  sites within the leaf. Ozone injury will not occur if
22             (1) the rate of O3 uptake is sufficiently small that the plant is able to detoxify
23             or metabolize O3  or its metabolites; or (2) the plant is able to repair or
24             compensate for the O3 impacts (Tingey and Taylor, 1982).  The uptake and
25             movement of O3 to the sensitive cellular sites are subject to various
26             physiological and biochemical  controls"  (U.S. Environmental Protection
27             Agency,  1986).
28
29           Responses to O3  exposure  that have been measured include reduced net CO2 exchange
30     rate (photosynthesis minus respiration), increased leaf/needle senescence, increased
31     production of ethylene, and changes in allocation patterns.  Overall understanding of the
32     response of plants to O3  has been refined since the last criteria document (U.S.
33     Environmental Protection Agency, 1986).   Increased emphasis has been placed on the
34     response of the process of photosynthesis to O3, on identification of detoxification
35     mechanisms, and on changes  in biomass (sugar, carbohydrate)  allocation.
       December 1993                           5_2i      DRAFT-DO NOT QUOTE OR CITE

-------
 1          As indicated above, entry of O3 into leaves involves the gas-phase external to the plant
 2     and the liquid—phase within the leaf cells.  A precondition for O3 to affect plant function is
 3     that it be absorbed into the tissues.  We will divide Oj uptake into two components,
 4     adsorption to surfaces and absorption into tissues. Adsorption will affect surface materials
 5     (e.g., cuticles, and have little direct affect on physiological processes), whereas
 6     O3 absorption can affect physiological function, if O3 is not first detoxified. In the following
 7     section the processes that control movement of O3 into the plant canopy and then into the
 8     leaf will be examined.
 9
10     5.3.2    Ozone Uptake
11          Uptake of O3 in a plant canopy is a complex process involving adsorption of O3 to
12     surfaces (stems, leaves, soil) and absorption into tissues, primarily leaves (Figure 5-2).
13     Movement of O3 from the atmosphere to the leaf involves micrometeoroloical processes
14     (especially wind) and the architecture of the canopy (including the leaves).  Within the
15     canopy O3 can be scavenged by chemicals in the atmosphere (Kotzias et al., 1990; Gab
16     et al.,  1985; Becker et al., 1990; Yokouchi and Ambe, 1985; Bors et al., 1989; Hewitt
17     et al.,  1990) however the products of these reactions may themselves be phytotoxic (Kotzias
18     et al.,  1990; Gab et al., 1985; Becker et al., 1990; Hewitt et al., 1990). The extent to
19     which  these scavenging processes affect O3 absorption by leaves is not well known.
20     Absorption of O3 by leaves is controlled in large part by canopy and leaf conductances.  The
21     former is a shorthand for the complex of microclimate and canopy architecture that control
22     movement of O3 from the bulk air to the leaf. Leaf conductance is determined by leaf
23     boundary layer conductance and stomatal conductance.  In this section we will examine
24     theoretical and empirical studies on O3 uptake at the canopy and leaf levels.
25
26     5.3.2.1   Ozone Uptake by Plant  Canopies
27          Integration of O3 uptake at the stand level requires attention to several levels of
28     organization (Enders et al., 1992; Hosker and Lindberg,  1982), because uptake at this level
29     includes not only absorption by leaves, but adsorption by stems, the soil, and other structures
30     with which O3 can react. While the actual pathway, and therefore conductance, will vary
31      within the canopy depending on position and wind profile, an integrated average conductance

        December 1993                           5-22      DRAFT-DO NOT QUOTE OR CITE

-------
          Atmospheric Processes
->/ Ozone in  1
  I atmosphere]
 I   Canopy
 I Boundary Layer
             Leaf Processes/
              Mode of Action
              Plant Response
           Ecosystem Response
                                                         Canopy
                                                       Conductance
                                             Ozone in
                                             Vegetation
                                              Canopy
                                                               IStomatal
                                                             Conductance!

      Figure 5-2.  Uptake of O3 from the atmosphere.  Ozone is moved from the atmosphere
                  above the canopy boundary layer into the canopy primarily by turbulent
                  flow of air.  Canopy conductance, controlled by the complexity of the
                  canopy architecture and the wide distribution within the canopy, is a
                  measure of the ease with which gases move into the canopy. Within the
                  canopy, O3 can be adsorbed by surfaces as well as being absorbed into the
                  foliage.  Foliage absorption is controlled by two conductances, leaf
                  boundary layer and stomatal, which together determine leaf conductance.
                  Solid black arrow denotes O3 flow; gray stipled arrows connect factors and
                  processes that affect O3 flow; open arrows connect major  processes.
                  Shaded boxes at the left are those processes described in the figure. The
                  shaded rounded box is end of pathway on this figure.
1     is frequently used to describe canopy conductance (Monteith and Unsworth, 1990).  For most

2     tree species canopy conductance tends toward high values while for crops it tends to be low.

3          Two general  approaches have been used to estimate O3 uptake by a plant stand:
4     (1) measurement of gradients over the canopy using micrometeorological methods and
      December 1993
       5-23
DRAFT-DO NOT QUOTE OR CITE

-------
 1     (2) simulation of canopy conductance.  The results of the two methods are generally different
 2     because the micrometeorological techniques include O3  uptake by all surfaces whereas
 3     simulation only accounts for O3 absorbed by the surfaces simulated, primarily the foliage.
 4          Two micrometeorological methods, Bowen ratio and eddy correlation, have been used
 5     to calculate canopy O3 uptake.  The Bowen ratio assumes a constant relationship (the Bowen
 6     ratio) between heat and water vapor fluxes (i.e., sensible and latent heat), then calculates
 7     O3 uptake assuming a constant relation between water vapor and O3 fluxes (Leuning et al.,
 8     1979a).  The eddy correlation  technique requires more elaborate instrumentation for
 9     measurement of variation in temperature, water vapor, and O3 concentration over time and
10     has stringent site requirements (Weseley et al.,  1978).
11          Wesely et al.  (1978),  using eddy correlation,  found a strong diurnal variation in the
12     deposition velocity  (the inverse of canopy conductance) and Oj flux over a corn canopy.
13     They also found evidence that 20 to 50% of the flux was to the soil and to the surface  of the
14     canopy.  Ozone flux to a dead corn canopy also had a diurnal variation, but a lower
15     magnitude, probably reflecting the absence of uptake through the response.  Single time
16     measures of deposition velocity,  or canopy resistance, have been taken in a Gulf Coast pine
17     forest (54 s m" ; Lenschow et  al.,  1982) and in a New Jersey pine forest (120 and
18     300 s cm  •. Greenhut. 1983.  Ozone uptake in a maple  forest varied diurnally in a pattern
19     explainable by variation  in  leaf conductance and O3 concentration (Fuentes et al., 1992).
20     Ozone flux below the tree canopy at 10 in was  about 10% of the flux above the canopy at
21     33 m.  Measurements in specially constructed chambers showed that O3 uptake, as well as
22     photosynthesis, could occur when the foliage was  wet (Fuentes and Gillespie, 1992). The
23     fact that wet leaves could take up significant CO2 is evidence that the response were not
24     blocked by the water on the leaf surface. This  result is counter to assumptions made in
25     earlier work (Baldocchi et al., 1987) in which water on  the surface of the leaf was presumed
26     to interfere with O3 uptake.
27          Simulation of canopy conductance requires scaling uptake from individual leaves to
28     individual trees to that of a stand using a combination of canopy models  (one for each
29     species)  and a stand model to  handle interactions among individuals.  Several assumptions
30     are required for this approach: (1) the primary sink for O3 is the foliage, (2) variation in
31     stomatal conductance can be simulated through  the canopy using either direct measurements

       December 1993                           5-24       DRAFT-DO NOT QUOTE OR CITE

-------
 1     or models, and (3) canopy/plant models adequately simulate response when competition is
 2     occurring.
 3          Leuning et al. (1979a,b) used a simple model to estimate canopy uptake in corn and
 4     tobacco. Comparison of the  results of these simulations with estimates using the Bowen ratio
 5     technique indicated that about 50% of the O3 absorbed by the stands entered the leaves.
 6     Baldocchi et al.  (1987) presented a model for canopy uptake of O3 that incorporated stomatal
 7     function, some aspects of canopy architecture, and soil uptake. The results of the simulation
 8     of O3 uptake by a corn canopy correlated well with estimations using the Bowen ratio,  but
 9     tended to overestimate the magnitude.  These authors point out that results of model
10     simulation  are quite sensitive to the assumptions used.  As part of a series of simulations,
11     Reich et al. (1990) explored the effects of different O3 exposures (daily average
12     O3 concentrations of 0.035, 0.05, 0.065, and 0.080 ppm) on canopy carbon gain in a mixed
13     oak-maple forest.  Depending on the response function and O3 exposure used, reductions in
14     carbon gain were between 5 and 60%.  An important result of these simulations is that the
15     effect of O3 was strongest in  the upper layer of the canopy, where most of the photosynthesis
16     occurred.  While all these simulations provide some interesting insights into how O3 uptake
17     (and response) varies with time and exposure, data for validating the models is  still needed.
18          In summary, O3 uptake (absorption to surfaces and absorption by tissues)  by plant
19     canopies has been measured only a few  times. The results are consistent with the hypothesis
20     that stomatal conductance plants a major role in the process.  Modelling of O3 absorption by
21     leaves provides a means of assessing our understanding of the processes controlling
22     O3 absorption.  Combining direct measurements over canopies with modelling will provide a
23     means for assessing the dynamics of O3 uptake in a canopy.
24
25     5.3.2.2  Ozone Absorption by Leaves
26          The importance of stomatal conductance for the regulation of O3 uptake by a canopy
27     has been hypothesized for some time (Heck et al., 1966; Rich et al., 1970).  Absorption of
28     O3 by leaves is primarily controlled by stomatal conductance which varies as a  function of
29     stomatal aperture (Figure 5-3). Kerstiens and Lendzian (1989) found that the permeability to
30     O3 of cuticles from several species was  about 0.00001 that of open response. Movement of
31     guard cells, which control stomatal opening, are affected by a variety of environmental

       December  1993                            5-25       DRAFT-DO NOT QUOTE OR CITE

-------
                  Light
        Humidity
      Figure 5-3.  Movement of gases into and out of leaves is controlled primarily by the
                  stomata—small openings in the. leaf surface whose aperture is controlled by
                  two guard cells.  Guard cells respond to a number of external and internal
                  factors, including light, humidity, CO2, water stress.  In general, the
                  stomata open in response to light and increasing temperature and close in
                  response to decreasing humidity, increased CO2, and increasing water
                  stress.  They may also close in response to  air pollutants, such as O3.
1     and internal factors, including light, humidity, CO2 concentration, and water status of the

2     plant (Zeiger et al., 1987; Kearns and Assmann, 1993). Air pollutants,  including O3, may

3     also affect stomatal function (U.S. Environmental Protection Agency, 1986).

4          For O3 to be absorbed by a leaf, O3 must be present in the atmosphere surrounding the

5     leaf, and the stomata must be open.  Any factor that affects stomatal opening affects

6     O3 absorption (Figure 5-3).  Under drought conditions when stomatal conductance is reduced

7     the relative effect of O3 is less when compared with well-watered controls (Tingey and
      December 1993
5-26
DRAFT-DO NOT QUOTE OR CITE

-------
 1     Hogsett, 1985; Flagler et al., 1987; Temple et al.,  1993, also see Section 5.4). Low
 2     humidity has been shown to modify plant response  to O3 (McLaughlin and Taylor, 1981),
 3     presumably due to reduced O3 absorption (Wieser and Havranek, 1993).
 4          To calculate O3 absorption, some estimate of the internal O3 concentration must be
 5     made.  In earlier work, a finite O3 concentration was assumed to exist in the intercellular air
 6     space of the leaf (Benett et al., 1973; Tingey and Taylor, 1982; Lange et al., 1989).
 7     Estimating this concentration is difficult because the rate of Oj absorption into the leaf must
 8     be known. Recently Laisk et al. (1989) presented evidence that this concentration is near
 9     zero, a result that is consistent with the highly reactive nature of O3.  Further studies  on
10     other species must be made to test the hypothesis that internal O3 concentration is negligible
11     in leaves.
12          The other component of absorption, O3 concentration outside the leaf, may vary greatly
13     with time of day and season (Chapter 4).  Data on  the effect of variations in O3 profile—
14     from constant concentrations to equal daily peaks to variable (episodic) peaks—suggest that
15     those profiles that have periodic high concentrations have a greater effect than those with low
16     peaks even though the exposure is equivalent (Hogsett et al., 1985a; Musselman et al., 1986;
17     see Section 5.6).  Taylor and Hanson (1992) show  how variations in conductance can affect
18     O3 absorption and conclude that conductances in and near the leaf surface have a major
19     influence on absorption of O3.  Figure  5-4 shows a simulation of the effect of diurnal
20     variation hi stomatal conductance and O3 concentration on the O3 absorbed into the leaf.
21     Amiro and Gillespie (1985) found that  cumulative O3 absorption correlated with visible
22     injury  in soybean.  Weber et al. (1993) found that rate of uptake may play an important role
23     in the response of ponderosa pine.  The roles of cumulative uptake versus uptake rate have
24     not been clarified and need further study.
25          Absorption of O3 by leaves depends on variations in both stomatal conductance and
26     O3 concentration.  The highly reactive  nature of O3 makes measuring its absorption difficult;
27     therefore, models of stomatal conductance are used along with O3 concentrations to estimate
28     O3 absorption.  The relative importance of absorption rate versus cumulative absorption is
29     not known at present.
30
31

       December 1993                           5-27      DRAFT-DO NOT QUOTE OR CITE

-------
                                  Ozone Profiles
                                       10    15
                                       Time (h)
                              20
                      -14:00 peak —12:00 peak-—16:00 peak —constant
                             Variation in Conductance
                                    Simulation
                                      10    15   20
                                      Time (h)
                                        B
                     *
                       10
                                Simulated Absorption
I
                     0)
                     §
                     &
                        6
                        *
                        ^
0
                  10     15
                 Time (h)
     20
                        - 14:00 peak —12:00 peak - -16:00 peak —constant
Figure 5-4. Simulation of the effects of diurnal variation in stomatal aperture and in
           O3 concentration on O3 uptake. A. Simulated conductance.  B. Diurnal
           O3 concentrations. C. O3 Uptake.
December 1993
                 5-28
DRAFT-DO NOT QUOTE OR CITE

-------
 1      5.3.3   Resistance Mechanisms
 2           Resistance mechanisms can be divided into two types:  (1) exclusion from sensitive
 3      tissue and (2) detoxification near or in sensitive tissue.  For leaves the former involve
 4      response and cuticles, and the latter various potential chemical and biochemical reactions that
 5      chemically reduce O3 in a controlled manner.  While these systems potentially provide
 6      protection against O3 damage to tissue physiology, they come at some cost, either in the
 7      reduction in photosynthesis in the case of stomatal closure or carbohydrate used to produce
 8      detoxification systems.
 9           Injury to leaf/needle cuticles does not appear to have a major affect on leaf function; at
10      least the data are not consistent. Barnes  et al. (1988) found that O3  exposure  could damage
11      leaf cuticles.  However Lutz et al. (1990) found no consistent changes in Norway spruce.
12
13      5.3.3.1   Stomatal Limitation
14           As noted above, response can be affected by a wide variety of environmental factors.
15      Some early research showed a decrease in leaf conductance (Figure 5-3) with  O$  exposure
16      implying a direct effect of O3  on stomatal conductance (U.S. Environmental Protection
17      Agency, 1986).  In studies at high O3 concentrations (>300 ppb) stomatal response was
18      rapid (Modlau et al., 1990).  In other studies reduction in conductance in response to
19      O3 required hours to days of exposure (Dann and Pell,  1989; Weber et al., 1993).  Several
20      studies have shown that discrimination against 13C in C3 plants decreases with
21      O3 fumigation (Okano et al., 1985; Martin  et al., 1988; Greitner and Winner  1988; Saurer
22      et al., 1991; Matyssek et al., 1992). These data are consistent with an increased restriction
23      to diffusion of CO2 into the leaf (Farquhar  et al., 1989).  However,  Matyssek et  al. (1992)
24      and Saurer et  al. (1991) found that internal CO2 increased with O3 exposure and  water use
25      efficiency decreased,  both the opposite of expectation, which indicates that photosynthesis
26      decreased relatively more than conductance. While response limit O3 uptake,  whether this
27      limitation results from direct effects of O3 on guard cell function,  indirectly through effects
28      on internal CO2 concentration,  or a combination has not be clearly demonstrated.
29
30
       December 1993                           5_29       DRAFT-DO NOT QUOTE OR CITE

-------
 1     5.3.3.2   Detoxification
 2          When O3 enters a cell,  several highly reactive compounds can be produced (e.g.,
 3     superoxide, free radicals, and peroxides) (Heath, 1987).  The effects of these compounds
 4     depends on their reactivity, mobility, and half-life.  For detoxification to occur oxidant and
 5     antioxidant must occur proximately. In addition, the rate of production of antioxidant must
 6     be a significant portion  of the rate of oxidant entry into the system of effective detoxification
 7     to occur.  Two general  kinds of detoxification systems have been reported in plants:
 8     (1) those that utilize reductants  (e.g., ascorbate) to reduce O3, and (2) those that utilize
 9     enzymes (superoxide dismutase). In either case excess oxidizing power is dissipated in a
10     controlled manner, effectively protecting the tissue from damage. These systems probably
11     developed to protect cells from photooxidation which can occur, for example, at low
12     temperatures (Powles,  1984).
13          Several antioxidants have  been reported, the most studied being ascorbate and
14     glutathione.  Much of this work has occurred since the 1986 criteria document (U.S.
15     Environmental Protection Agency,  1986).  Alscher and Amthor (1988) reviewed the
16     literature in this area.  In the chloroplast, the process requires NADPH and may be a cause
17     for the transient reduction in photosynthesis observed in  some studies (Alscher and Amthor,
18     1988).
19          Evidence for the participation of antioxidants in protecting cells from O3 injury is
20     primarily indirect  (i.e., changes in  levels of antioxidants or of associated enzymes). In red
21     spruce, glutathione levels increased in year-old needles in response  to O3, but not in current
22     year needles (Hausladen et al., 1990; Madamanchi et al., 1991). Dohmen et al. (1990)
23     found  increased concentrations  of reduced glutathione in Norway spruce in response to
24     long-term O3 fumigation. In a poplar hybrid, total glutathione increased with O3 fumigation;
25     however, the ratio of reduced to oxidized forms declined, indicating oxidation of glutathione
26     was possibly stimulated by O3  (Sen Gupta  et al.,  1991).  Mehlhorn et al. (1986) found that
27     both glutathione and ascorbic acid increased with O3 fumigation in  white fir (Abies alba)
28     and Norway spruce.  The potential for ascorbic acid to protect cells from O3 damage was
29     explored by Chameides (1989).  He concluded that such protection  was possible if ascorbic
30     acid occurred in the apoplast at sufficient concentrations and sufficient production rates;
31     however, experimental  data are needed to test the hypothesis.

        December  1993                            5-30        DRAFT-DO NOT QUOTE OR CITE

-------
 1          The response of enzymes involved in detoxification is not clear.  Activities of enzymes
 2     involved in antioxidant production increased in response to O3 in one study (Price et al.,
 3     1990); however, in several others no effect was found (Madamanchi et al., 1992; Pitcher
 4     et al.,  1991; Anderson et al., 1992; Nast et al., 1993). Activity of superoxide dismutase, an
 5     enzyme that can reduce one of the products of O3 interaction with the cytoplasm, can be
 6     increased by O3 fumigation (Alscher and Amthor, 1988; Sen Gupta et al.,  1991).  There are
 7     both cytosolic and chloroplastic forms of this enzyme, but the role the different forms plant
 8     in detoxification of O3 is not clear.  Teppermann and Dunsmuir (1990) and Pitcher et al.
 9     (1991) found that increased production of SOD had no effect on resistance to 63 in tobacco.
10          The extent to  which these detoxification systems can protect tissue from O3  damage is
11     unknown.  However, "If plants have detoxification mechanisms which are kinetically limited,
12     the rate of O3 uptake may be important, so that even an integrated absorbed dose may be
13     insufficient to account for observed  responses" (Cape and Unsworth,  1988).  Potential rates
14     of detoxification for given tissues are needed to estimate the importance of these systems to
15     overall O3 response.  In addition, the sites in which the detoxification systems occur need to
16     be identified.
17
18     5.3.4   Physiological Effects of Ozone
19          The initial reactions of O3 with cellular constituents are not known.  The high reactivity
20     and non-specificity  of O3 reactions coupled with the absence of a useful isotopic tag for
21     O3 make studies of the  initial reactions difficult at best.  The data on changes in biochemical
22     function resulting from  O3  exposure probably represent effects one or more steps beyond the
23     initial  reactions.  Nonetheless, we do have data which indicate the wide range of cellular
24     processes that can be affected by  O3.
25          Ozone that has not been neutralized by one of the detoxification systems (Figure 5-5)
26     acts first at the biochemical level  to impair the functioning of various cellular processes
27     (Tingey  and Taylor, 1982;  U.S. Environmental Protection Agency, 1986). The result of
28     these impairments are reflected in integrated changes in enzyme activities,  membrane
29     function, and energy  utilization (Queiroz, 1988).  Several related papers have shown that the
30     activity of the primary carboxylating enzyme (RuBP-carboxylase)  is reduced  by O3 exposures
31     in the  range of those  measured at some sites (Dann and Pell, 1989; Enyedi et al.,  1992; Pell

       December 1993                           5.31       DRAFT-DO  NOT QUOTE OR CITE

-------
        Atmospheric Processes
         Ecosystem Response
                                      Reduced
                                   Photosynthesis
           Leaf Processes/
            Ozone Uptake
                                             Physiological Response to Ozone
    Increased
     Foliage
  Senescence
           Repair
        Replacement
                                                Reduced Canopy
                                                  Carbohydrate
                                                   Production
                                                                           Respiratory
                                                                             Losses
      Figure 5-5.  Effects of O3 absorption into a leaf. Once inside the leaf Oj can have a
                  number of effects all of which affect carbohydrate production and
                  utilization.  Reduced photosynthesis, increased leaf senescence, production
                  of detoxification systems, and increased respiration (both maintenance and
                  growth) reduce the amount of carbohydrate available for allocation.
                  Compensation  through production of new leaves, for instance, can counter
                  some or all of these effects depending on the O3 exposure, physiological
                  state of the plant, and the species.  Integration of these processes leads to
                  changes in the amount of carbohydrate available for allocation from the
                  canopy.  Solid black arrows denote O3 flow; gray stipled arrows show the
                  cascade of effects of O3 absorption on leaf function.
1     et al., 1992; Landry and Pell, 1993).  Membrane injury has been found in some experiments

2     using acute levels of O3 (Heath, 1987).  Chronic exposure can lead to changes in lipid

3     composition and changes in cold resistance (Brown et al., 1987; Davison et al., 1987;

4     DeHayes et al., 1991; Lucas et al., 1988; Wolfenden and Wellburn, 1991).  Recently, Floyd
      December 1993
5-32
DRAFT-DO NOT QUOTE OR CITE

-------
  1      et al. (1989) have been shown that O3 can affect nuclear DNA through the formation of
  2      aducts.
  3           Changes  in the in vivo concentrations of various growth regulators in response to
  4      O3 exposure could have important consequences for plant function.  However, the effects of
  5      O3 on levels and activities of growth regulators have not been studied extensively.  Ozone
  6      has been shown to stimulate ethylene production and inhibitors of ethylene production have
  7      been found to reduce the effects of O3 in short-term experiments (Pell and Puente, 1986;
  8      Rodecap and Tingey, 1986; Taylor et al.,  1988; Mehlhorn et al., 1991; Telewski, 1992;
  9      Langebartels et al., 1991; Mehlhorn and Wellburn,  1987; Kargiolaki et al.,  1991; Reddy
 10      et al., 1993).   Ethylene is produced during ripening of fruit, during periods  of stress, and
 11      during senescence (Abeles et al., 1992). Increased levels of ethylene in the leaves could play
 12      a role in the early senescence of foliage.  In some cases there is a correlation between
 13      ethylene production and O3 sensitivity;  however, the relationship is complex and makes use
 14      of ethylene production as an index of sensitivity problematic (Pell, 1988).
 15           Abscisic acid plays  an important role in stomatal function (Davies et al., 1980).
 16      Atkinson et al. (1991) found that response from  O3 fumigated leaves were less sensitive to
 17      ABA than control leaves.  These data could explain the observation that stomatal function is
 18      unpaired by long-term O3 exposure.  Kobriger et al.  (1984) found no effect of O3 on
 19      whole-leaf content of abscisic acid, but  changes in compartmentation could not be ruled out.
20           Physiological effects of O3 uptake are manifest in two primary ways:  (1) reduced net
21      photosynthesis  and (2) increased senescence (Figure 5-5).  Both decreased photosynthesis and
22      increased leaf senescence result in the loss of capacity for plants to form carbohydrates,
23      thereby having a major impact on the growth of the plant (Figure 5-6).
24           Ozone-induced reduction in net photosynthesis has been known for some time  (U.S.
25      Environmental Protection Agency, 1986).  Changes in stomatal conductance, in
26      photosynthetic  capacity, carbohydrate allocation and respiration have been documented.  The
27      relationship between O3 exposure and photosynthesis is not well known. Photosynthesis
28      provides plants with the energy and structural building blocks necessary for their existence.
29      The photosynthetic capacity of a plant is an important aspect of plant response to stresses in
30      natural environments and  is strongly associated with leaf nitrogen content and with water
       December 1993                           5.33      DRAFT-DO NOT QUOTE OR CITE

-------
         Atmospheric Processes
           Canopy Processes
            Leaf Processes/
             Ozone Uptake
            Leaf Processes/
             Mode of Action
          Ecosystem Response
Carbohydrate
Allocation
i
\
                               f Compensation
      Figure 5-6. Effect of O3 on plant function and growth.  Reduction in carbohydrate
                  allocation affects the pool of carbohydrates available for growth.  Changes
                  in relative growth rate of various organs as a function of O3 exposure
                  suggest that allocation patterns of carbohydrate is affected.  Solid black
                  arrows denote where O3 absorption affects the allocation processes of the
                  plant; gray stipled arrows show the cascade to  plant growth.
1     movement.  Both resources are essential if the process is to occur and involves the allocation
2     of carbohydrates from the leaves to the roots for nitrogen acquisition and water uptake.  Leaf
3     photosynthetic capacity is also age dependent. As the plant grows, the canopy structure
4     changes altering the amount and angle of light hitting a leaf.  Allocation of carbohydrates and
5     nutrients to  new loaves is especially  important in stimulating growth production (Pearcy
6     et al., 1987).  Reductions in photosynthesis are likely to be accompanied by as shift in
7     growth pattern which favors shoots and by an increase or decrease in life span (Winner and
8     Atkinson, 1986). Therefore, alteration of the processes  of photosynthesis and carbohydrate
       December 1993
5-34
DRAFT-DO NOT QUOTE OR CITE

-------
  1      allocation affects plant response to stresses such as O3. Reduction in photosynthesis, reduced
  2      carbohydrate formation and allocation to leaf repair or to  new leaf formation decreases the
  3      availability of carbohydrates, alters the normal allocation pattern and, therefore, all aspects
  4      of plant growth and reproduction (Figure 5-6).  The effects of a reduction in photosynthesis
  5      on growth and reproduction was discussed in the previous criteria document (U.S.
  6      Environmental Protection Agency,  1986).
  7           Carbohydrate production  by a single plant is controlled not only by photosynthetic
  8      capacity of the foliage but also by the amount and distribution of that foliage.  Stow et al.
  9      (1992) and  Kress et al.  (1992)  found that O3 exposure affected needle retention in loblolly
10      pine.  Similar data have been reported for slash pine (Byres et al., 1992).  Keller (1988) and
11      Matyssek et al.  (1993a,b) reported increased senescence with increased  63 exposure in
12      aspen,  as did Wiltshire et al. (1993) in apple.  Replacement of injured leaf tissue has been
13      reported for some species when they  are exposed to low O3 concentrations (Held et al.,
14      1992; Temple et al., 1993).  Temple et al. (1993) also found increased photosynthetic
15      capacity of new needles in O3 treatments compared to  controls.
16           Few direct effects of O3 have been found outside leaves.  Kargiolaki et al. (1991) found
17      that intumescences appear on stems of poplar after 72 days of O3 fumigation (70 to 80 ppb).
18      Ozone probably enters the stem through the lenticles that occur on the surface of the stem
19      and allow direct exchange of gases between the stem and the air.  The consequence of this
20      response to O3 is not clear; however, it may be related to the reduction in phloem transport
21      rate observed in loblolly pine (Spence et al., 1990).
22
23      5.3.4.1  Carbohydrate Production and Allocation
24           The importance of photosynthesis and carbohydrate allocation in plant growth and
25      reproduction has been pointed out previously.  The patterns of carbohydrate allocation
26      directly affect growth rate.  Plants require a balance of resources  to maintain optimal growth,
27      however, in natural environments optimal conditions seldom occur.  Therefore, plants must
28      compensate for differences in resource availability as well as for environmental stresses.
29      They do this by changing the way they allocated carbohydrates (Chapin  et al., 1987). Each
30      response to stress affects the availability of carbohydrates  for allocation  from the leaves
31      (Figure 5-5).  The carbohydrate pool  is affected both by a reduction in the carbohydrate

        December 1993                           5.35       DRAFT-DO NOT QUOTE OR CITE

-------
 1     produced and by a shift of carbohydrate to repair and replacement processes. The effect is
 2     particularly noticeable in the roots where O3 exposure significantly reduces available
 3     carbohydrate (Andersen et al., 1991; Andersen and Rygiewicz, 1991).  Effects on leaf and
 4     needle carbohydrate content have ranged from a reduction (Barnes et al., 1990; Miller et al.,
 5     1989), to no effect (Alscher et al., 1989), to an increase (Luethy-Krause and Landolt, 1990).
 6     Cooley and Manning  (1987) reviewed the literature on carbohydrate partitioning and noted
 7     that "storage organs...are most affected by O3-induced partitioning changes when
 8     O3 concentrations are in the range commonly observed in polluted ambient air."
 9          The above discussion supports the information in the previous criteria document (U.S.
10     Environmental  Protection Agency, 1986), which pointed out that roots were usually more
11     affected by O3  exposures than the shoots.  Studies by Miller et al. (1969), Tingey et al.
12     (1976a), McLaughlin et al. (1982) and Price and Treshow, (1972) were cited in support of
13     the view.  Miller et al.,  noted reduction in photosynthesis was accompanied by decreases in
14     sugar and  polysaccharide fraction in injured needles of ponderosa pine seedlings and altered
15     allocation of carbohydrates. Exposure were for 30 days, 9 h/day to concentrations of 0.15,
16     0.30 or 0.40 ppm.  These exposures reduced photosynthesis by 10, 70 and 85%,
17     respectively. The observations of Tingey et al. (1976) indicated that O3 exposures
18     differentially affected metabolic  pools in the roots and tops of ponderosa pine seedlings
19     grown  in field. Further, this study indicated that the amounts of soluble sugars, starches,
20     and phenols tended to increase in the tops and  decrease in plant roots of ponderosa pine
21     seedlings exposed to 0.10 ppm O3 for 6 h/day  for 20 weeks.  The sugars and starched stored
22     in the tree roots were significantly less than those in the roots of controls.  In another study
23     cited in the 1986 document, McLaughlin et al. (1982) also observed the reduced availability
24     of carbohydrate for allocation to the roots and  stated that the result was reduced vigor and
25     enhanced susceptibility of trees to root diseases.  Loss of vigor was due to a sequence of
26     events, including premature senescence and loss of older needles, lower gross photosynthetic
27     productivity, and reduced photosynthate (carbohydrates) available for growth and
28      maintenance, that were associated with exposure to O3.  Carbon-14 transport patterns also
29      indicated changes in  carbon allocation. Older  needles were found to be the source of
30      photosynthate  for new needle growth in the spring and were storage sinks in the fall.
        December 1993                           5-36      DRAFT-DO NOT QUOTE OR CITE

-------
 1      Retention of l4C-pholosynthale by foliage and branches of sensitive trees indicated that
 2      allocation to the trunks and roots was reduced.
 3           Lost carbohydrate production has effects throughout the plant (Figure 5-6).  The roots
 4      and associated mycorrhizal fungi are especially  susceptible to reduced carbohydrate
 5      availability and quite frequently show the greatest decline in growth (Adams and O'Neill
 6      1991; Edwards and Kelly, 1992; McQuattie and Schier, 1992; Meier et al.,  1990; Taylor and
 7      Davies, 1990).  However, in some cases, increased mycorrhizal formation has been reported
 8      (Goriseen et al., 1991; Reich et al.,  1985).  It might be expected that reduced allocation to
 9      roots would affect shoot growth through  increased susceptibility to water stress, reduced
10     nutrient availability (Flagler et al., 1987), and reduced production of growth factors (Davies
11      and Zhang, 1991;  Letham and Palni, 1983). Effects on production and retention  of leaves
12     and needles were described above.  Effects on stem growth have been found in tree species
13     (Hogsett et al.,  1985b; Mudano et al., 1992; Pathak et al., 1986; Matyssek et al., 1992;
14     Matyssek et al., 1993b).   Changes in canopy density, root/shoot ratio, and stem growth will
15     affect the functioning of the plant and may make plants more susceptible to environmental
16     stresses, such as drought and nutrient limitation, that are characteristic of many ecosystems.
17
18     5.3.4.2   Compensation
19          Compensatory responses occur as plants attempt to minimize the effects of stress.
20     Responses include adjustments to changes in physiological processes (e.g., photosynthetic
21     capacity and foliage production) that tend to counteract the effects  of O3 absorption by the
22     leaves.   Pell et al. (in press)  have reviewed the extensive literature produced in the ROPIS
23     experiment.  A wide range of compensatory responses have been identified, especially
24     reallocation of resources leading to increased relative growth in the shoot  compared to the
25     root (see above).  Compensation can take the form of production of new tissue (e.g., leaves)
26     to replace injured  tissue and/or biochemical shifts, including increased photosynthetic
27     capacity in new foliage.
28          Changes in respiratory  rate have been attributed to such repair processes (U.S.
29     Environmental Protection Agency, 1986).  Recent studies  have found stimulation  of dark
30     respiration in Norway spruce (Barnes et  al., 1990; Wallin et al., 1990) and bean  (Amthor,
31      1988; Amthor and Gumming, 1988; Moldau et al., 1991).  Repair of membranes (Sutton and

       December 1993                           5-37       DRAFT-DO NOT QUOTE OR CITE

-------
 1     Ting, 1977; Chevrier et al., 1988, 1990) and of injured enzymes are two probable reasons
 2     for increased respiration.  Ozone has been shown to increase the ATP/ADP ratio, which is
 3     consistent with increased respiratory activity (Weidmann et al., 1990; Hampp et al., 1990).
 4     As in the case of detoxification, the importance of repair processes in the overall
 5     carbohydrate budget of the plant and of their influence of apparent threshold is unknown.
 6          Recovery of photosynthetic capacity after O3 exposure has been noted in some studies.
 7     Early work indicated that recovery of photosynthetic capacity could occur after exposure of
 8     high concentrations (>0.25 ppm) of O3 (e.g., Botkin, 1971, 1972).  Dann and Pell (1989)
 9     found that photosynthetic rate, but not Rubisco activity, recovered within a few days in
10     potato after exposure to 0.2 ppm O3.  In ponderosa  pine, photosynthetic rates in O3 treated
11     needles  recovered to that of controls within 40-50 days (Weber et al., 1993).  To what
12     extent this recovery can offset losses in  carbohydrate gain is not known nor is the
13     mechanism.
14          Replacement of injured foliage (see Section 5.3.4) is another method to  counteract the
15     effects of O$ exposure.  The extent to which increased leaf/needle production and increased
16     photosynthetic capacity in the new foliage compensates for O3 injury is not known.
17          The importance of various compensation mechanisms is not sufficiently  well-known to
18     allow an estimate of the degree to which they might mitigate the effect of O3. The fact that
19     increases in photosynthesis and in leaf production have been measured indicates that these
20     processes, at least, may be important.
21
22     5.3.5  Role of Age and Size Influencing Response to Ozone
23          Plant age, physiological state of growth and the frequency to which plants are exposed
24     play an  important role in plant response to O3.  In annual species, effects of O3 exposure can
25     result in a reduction in the amount and size of seed  production through changes in allocation
26     that occur over the years.  In perennial  species, reduced growth occurs due to a reduction in
27     the amount of carbohydrates available for storage.  In both cases, carbohydrates will have
28     been used to help the plants minimize the stress of O3 exposure. It should also be noted that
29     in absence of O3 exposure, in hardwoods leaf photosynthetic capacity reaches an early peak
30     and then gradually declines until senescence. Conifers, on the other hand retain leaves
31     longer than one  year (Pye, 1988).

       December 1993                           5-38      DRAFT-DO NOT QUOTE OR CITE

-------
 1           Carry over effects of O3 have been documented in growth of tree seedlings (Hogsett
 2     et al., 1989; Sasek et al., 1991; Temple et al., 1993) and in regrowth of roots (Andersen
 3     et al., 1991). Accumulation of these effects will affect survival and ability to reproduce.
 4     Data on cumulative effects of multiple years of O3 exposure are extremely limited (Kress
 5     et al., 1992; Hogset et al., 1989).  Controlled exposures have been for the most part 2 to
 6     3 years.
 7           A tacit assumption in much of the research on Oj effects on trees is that seedling
 8     response to O3 is a good predictor of large  tree  response.  This assumption has been
 9     necessitated by the difficulty in exposing large trees for long times to Oj.  Pye (1988)
10     reviewed the problems of extrapolation from seedling/sapling experiments to large trees and
11     noted several areas of difference between seedling/saplings and large trees.  The problems
12     include not only size but are those equivalent to a single tree growing in a field and a tree
13     growing in a stand. There exists, between  seedlings and large trees, a difference the ratio of
14     photosynthetic to respiratory tissue;  as a tree ages, the photosynthetically inactive tissue
15     grows.   Cambial tissues associated with stem, branch, and coarse roots also increase.
16     Another difference is the existence of microclimatic and morphologic gradients across a
17     canopy and altered water and nutrient regimes.  Deep forest canopies generate a
18     microclimatic gradient that is paralleled by  a morphological gradient from sun leaves to
19     shade leaves. Associated with this gradient is net radiation, which can vary by an order of
20     magnitude within the canopy.  Windspeed and air temperature  decrease from above to below
21     the crown,  while air humidity and CO2 increase.  Ozone concentrations could also vary with
22     forest crown depth, however, measurements have not been made. Cregg et al. (1989) also
23     argue that these differences in scale can affect growth responses seen.   Some studies have
24     indicated that seedlings may be more sensitive (i.e., greater visible injury) than large trees
25     (Kozlowski, Kramer, and Pallardy,  1992); however, Samuelson and Edwards (in press) have
26     found that leaves on large red oak trees are more sensitive than those on seedlings.  It is
27     likely that a variety of factors determine sensitivity to O3, including stomatal function and
28     presence of detoxification systems, so that in some cases seedlings will be more sensitive and
29     in others large trees will. While each of  the four differences between  small and large trees
30     mentioned above can be supported on theoretical grounds, little direct information is
31     available to evaluate the importance of these differences, especially with respect of O3.

       December 1993                           5.39      DRAFT-DO NOT QUOTE OR CITE

-------
 1          The microclimate of the canopy of mature trees is quite different from that of seedlings.
 2     Radiation intensity through the multilayer canopy can vary by an order of magnitude or more
 3     can be expected (Jones, 1992). In addition, gradients of other important microclimatic
 4     variables  (temperature, humidity, wind speed) exist within the canopy. These will all affect
 5     stomatal conductance and some (e.g., wind speed), will affect canopy conductance.
 6          The effect of size on transport processes and the subsequent response to O3 is
 7     unknown.  The simple fact of greater distance over which transport must occur will affect the
 8     timing of response of organs distant from the primary site of O3 impact,  the foliage.   Studies
 9     using methods  that integrate functions over the whole tree could provide useful information.
10     For example, combinations of porometer measurements on foliage and whole plant water use
11     measured (Schulze et al., 1985) on individuals of different sizes could provide very useful
12     information on the coupling of leaf level processes to whole canopy and whole plant
13     response.  Greater evaporative demand in large than small trees as the result of greater leaf
14     area and different microclimate could lead to transient water stress and stomatal closure,
15     because of insufficient water transport capacity.
16           As a tree grows from a seedling to a large tree the ratio between photosynthesis and
17     respiration declines as a  greater portion of the plant tissue is non-photosynthetic.  It is
18     reasonable to assume that such a change could result in less resource  being available for
19     detoxification and repair as the plant grows.  How this change affects the ability of a plant to
20     survive O3 (or any other stress) is not known.  Recently, Samuelson and Edwards (in press)
21     present data on northern red oak that show O3 decreased photosynthetic capacity more on
22     lower leaves within the canopy of large trees than on leaves near the  top of the canopy—
23     a result apparently counter to the model  results of Reich et al. (1990). Seedling
24     photosynthesis  was not affected by the same O3 exposure.  A more interesting result of this
25     work is the reduction in total canopy biomass found in large trees exposed to O3.  It is not
26     possible to directly assess the relative importance of reduced photosynthesis versus loss of
27     canopy from these data, but they do show that differences may exist between large trees and
28      seedlings in their response to O3.  These differences may be due to changes in carbon
29      budgets,  stomatal characteristics, microclimate, and flushing patterns  that develop as
30      seedlings become trees.  The ability of northern red oak seedlings to  produce three flushes
        December 1993                            5-40      DRAFT-DO NOT QUOTE OR CITE

-------
 1     and thus replace injured foliage may be an important defense mechanism in the seedling
 2     stage.  The generality and physiological basis of these findings need further investigation.
 3          In evergreen perennial plants, foliage must be maintained from one year to the next,
 4     frequently through periods unfavorable to growth. In evergreen species that retain a few to
 5     several years of leaves increased susceptibility to stress  (e.g., frost) could further reduce
 6     potential canopy photosynthesis in subsequent years (Brown et al., 1987; Davison et al.,
 7     1987; DeHayes et al.,  1991; Lucas et al., 1988).  Fincher (1993) found that O3 decreased
 8     frost tolerance in red spruce in both seedlings and trees. The consequences of this change to
 9     seedlings and large trees is in need of further work.
10          The effect of O3 on storage of carbohydrates in large compared to small trees is  not
11     known.  Changes in storage could affect the ability of the plant to withstand other stresses
12     and/or to produce adequate growth during each  growing season.
13           Dendrochronology (tree-ring analysis) provides the opportunity to do retrospective
14     studies over the leaf of large trees.  Reduction in annual radial growth has been found in the
15     southern Sierra Nevada for Jeffrey pine but not  for ponderosa pine (Peterson et al., 1987;
16     1989, 1991; Peterson and Arbaugh,  1988).  One difficult with using tree-ring data to
17     estimate O3-related effects is that it is not always possible to separate reductions due to
18     O3 from other effects (e.g., drought).
19          Development of reliable methods for scaling from small to large trees are crucial to the
20     prediction of the long-term effects of O3 on forest function. Measurement of the response of
21     different size trees to O3 could provide useful data on the relative responses of small and
22     large trees.  However, problems exist in giving  similar  exposures to trees of widely different
23     sizes.  The most direct method is to fumigate trees over a significant portion of their life
24     span.  Time is the primary obstacle to these studies because they would require decades to
25     complete.  Whatever methods are used must be  based on a good understanding of the
26     physiological changes that occur as trees grow.
27
28     5.3.5.1   Summary
29          In the previous criteria document it was concluded that the "Critical effects, including
30     reduction in photosynthesis and a shift in the assimilation of photosynthate, will lead to
31     reduced biomass, growth, and yield" (U.S.  Environmental Protection Agency,  1986).

       December 1993                           5-41       DRAFT-DO NOT QUOTE OR CITE

-------
 1     In addition, changes in carbohydrate allocation patterns and affects on foliage were noted as
 2     important.  Since that report additional information has been developed, especially on the
 3     effects of O3 on photosynthetic capacity.  However, at present there is still no clear
 4     understanding of the initial biochemical changes resulting within the leaf cells after the entry
 5     of O3 and how these changes interact to produce the observed responses.  Much of the
 6     earlier research used very high (0.25 ppm or greater) O3 concentrations which produced what
 7     could be characterized as acute responses. More recent research has used lower
 8     concentrations, usually including near ambient O3 level, so that the observed responses may
 9     be more relevant to field conditions.  One characteristic of these more recent data is that a
10     longer exposure (days to weeks instead of hours) is needed to show a response.
11          As a result of the research since the last criteria document, we have a better
12     understanding of the reduction of photosynthesis as a result of O3  exposure, especially its
13     affects on the central carboxylating enzyme (ribulose-6-P-carboxylase/oxygenase).  The rate
14     of senescence of leaves has been shown to increase as a function of increasing O3 exposure.
15     At near-ambient exposures, leaf production has been shown to increase in some species,
16     thereby off-setting  the increased loss to due senescence.  The mechanism of the increase in
17     senescence  is not known at the present time and deserves further study.  Finally, the role that
18     changes in  allocation of resources plays in plant response to O3 has gained greater
19     prominence.  Most studies have shown that allocation  of photosynthate to roots  is decreased
20     by O3. In  some cases, allocation to leaf production has increased.  Whether these changes
21     are driven entirely  by changes in carbohydrate availability or are controlled by other factors
22     (e.g., hormones) is not known at present.
23           Some potentially significant processes have been investigated since the last Criteria
24     Document, especially detoxification and compensatory processes.  The role(s) of
25     detoxification in providing a level of resistance to O3 has been investigated; however, it is
26      still not clear to what degree these processes can provide protection against O3  damage.
27     Data are  especially needed on the potential rates of antioxidant production and on the
28      subcellular localization of the antioxidants. Potential rates of antioxidant production are
29      needed to assess whether they are sufficient to detoxify the O3 as it enters the cell.  The
30      localization is needed to assess whether the antioxidants are in a location (cell wall or
31      plasmalemma) which  permits contact  with the O3 before it has a chance to damage

        December  1993                            5-42       DRAFT-DO NOT QUOTE OR CITE

-------
  1     subcellular systems.  Ozone exposure has been shown to decrease cold tolerance of foliage in
  2     some species.  This response could have a major impact on long-lived evergreen species that
  3     retain leaves for several years.  Various forms of compensation, especially stimulation of
  4     production of new leaves and higher photosynthetic capacity of new leaves, have been
  5     reported.  While these processes divert resources away from other sinks, compensation may
  6     counteract the reduction in canopy carbon fixation produced by O3.  The quantitative
  7     importance of these processes is still in need of investigation.  At the canopy level some
  8     additional evidence that diurnal stomatal variation is important in O3 uptake.  These data will
  9     provide important checks on the modelling of stand response to O3.
 10          Questions  still  remaining to be addressed include: How does the plant accumulate the
 11     effects  of O3 absorption?  How important are cumulative O3 absorption and O3 absorption
 12     rate? How does the plant integrate injury due to O3 absorption, detoxification,
 13     compensation, and other processes into a whole-plant response?  What are the roles of
 14     growth regulators, especially ethylene?  Are they significant?  The major problem facing
 15     researchers trying to predict long-term O3 effects on plants is how the plant integrates all of
 16     the response to O3 into the overall response to the environment, including naturally occurring
 17     stresses.  Little is now known about how response to O3 changes with increasing age and
 18     size.  This information is crucial to predicting the long-term consequence of O3 exposure in
 19     forested ecosystems.
 20
 21
 22     5.4   FACTORS THAT MODIFY PLANT RESPONSE
 23     5.4.1   Modification of Functional and Growth Responses
 24          Plant response  to oxidants may be modified by various biological, physical, and
 25     chemical  factors. Biological factors that modify plant response include those within the plant
 26     as well  as those  external to the plant.  The genetic make up as well as their development
 27     stage play critical roles in the way  individual plants respond to O3 and other external
28     stresses.  For example, different varieties or cultivars of a particular species are known  to
29     differ greatly in  their response to a given exposure to O3, while the magnitude of the
30     response of a particular variety, in  turn,  depends upon environmental factors such as
31      temperature and  humidity, soil  moisture and nutrition, the presence of pests or pathogens,

        December 1993                           5.43      DRAFT-DO NOT QUOTE OR  CITE

-------
 1     and exposure to other pollutants or agricultural spray chemicals.  In other words, response
 2     will be dictated by the plant's present and past environmental milieu,  which also includes the
 3     temporal pattern of exposure, and the plant's stage of development.  The corollary is also
 4     true:  exposure to oxidants can  modify response to other environmental variables.  For
 5     example, exposure to O3 reduces the ability of trees to withstand winter injury caused by
 6     exposure to freezing temperatures (Davison et al.,  1988), and influences the success of pest
 7     infestations (Hain, 1987; Lechowiez, 1987).  Hence, both the impact of environmental
 8     factors on response to oxidants  and the effects of oxidants on responses to environmental
 9     factors have to be considered in determining the impact of oxidants on vegetation in the field.
10     These interactions are summarized as the involvement of "other stresses" in the scheme
11     shown in Figure 5-6 (Section 5.3).  In the following review, the environmental factors are
12     grouped into three categories:  biological (including genetic and developmental components),
13     physical, and chemical.
14           Runeckles and Chevone (1992) have recently provided a general review  of the
15     interactive effects of environmental  factors and O3. The subject is also treated in a National
16     Acid  Precipitation Assessment Program report  (Shriner et al., 1990).
17
18     5.4.2   Genetics
19           The response of an individual  plant within a species and at a given age is affected both
20     by its genetic makeup and the environment in which it grows.  This section examines the role
21     of genetics in plant response to O3 and its implication for both managed and natural
22     ecosystems.  In addition,  major knowledge gaps in the understanding of genetic  aspects of
23     O3 responses are pointed  out.
24           The responses of plants to O3  are strongly influenced by genetics  as was summarized in
25     the air quality criteria document for O3 (U.S. Environmental Protection Agency, 1986).
26     Thus, the plants of a given population or family will not respond to O3 in the same way,
27     even  if they are grown in a homogenous environment.  This has been amply demonstrated
28     through intraspecific comparisons of O3 sensitivity as determined by  foliar sensitivity of
29     ornamental plants, the aesthetic value of which are decreased by visible foliary injury, and of
30      woody plants that are  important components of natural  ecosystems (Table 5-1).  Ornamental
31     plants and plants growing in wilderness areas, for example, have an intrinsic  worth, apart

       December 1993                           5-44       DRAFT-DO NOT QUOTE OR CITE

-------
       TABLE 5-1.  EXAMPLES OF INTRASPECIFIC VARIATION OF FOLIAR
                            SYMPTOMS IN OZONE RESPONSE
Species
Ornamental,
Non-Woody
Plants
Petunia sp.
(Pentunia)
Poa pratensis L.
(Kentucky bluegrass)
Genetic
Unit"



Cultivars
Cultivars
Concentration



400 ppb -
4 h/day
400 ppb
300 ppb
Duration



4 days
2h
4h
Range of
Response



20 to 60% (3)
0 to 90%(3)
30 to 60% (3)
Reference



Elkiey and Ormrod
(1979)
Murray et al. (1975);
Wilton et al. (1972)
 Trees
 Acer rubrum L.
 (Red maple)
 Fraxinus americana L.
 (White ash)
Populations

Half-sib
families
 Fraxinus pennsylvanica   Half-sib
 Marsh. (Green ash)      families
 Gleditsia triacanthos L.   Cultivars
 (Honeylocust)
 Pinus ponderosa         Half-sib
 Dougl. ex  P.            families
 Laws and C. Laws
 (Ponderosa pine)
 Pinus strobus L.         Clones
 (Eastern white pine)
 Pinus taeda L.           Half-sib
 (Loblolly pine)           families

 Populus tremuloides      Clones
 Michx. (Trembling
 aspen)
750 ppb
7 h/day
500 ppb
250 ppb

500 ppb
250 ppb
            Ambient

            1.5 x ambient




            300 ppb

            250 ppb
            ambient +
            60 ppb
            200 ppb
            150 ppb
3 days

7.5h
6h

7.5 h
6h
19 to 34%(2)

0 to 50% (3)
2 to 33% (2)

0 to 40%(3)
2 to 39% (2)
               1 growing  0 to 34% (3)
               season
               3 growing  0 to 28% (2)
               seasons
               6h
               8 h        3 to 29% (2)
               1 growing  1 to 42% (1)
               season
Townsend and
Dochinger (1974)
Karnosky and Steiner
(1981); Steiner and
Davis (1979)
Karnosky and Steiner
(1981);
Steiner and Davis
(1979)
Karnosky (198 la)

Temple et al. (1992);
           0 to 60% (3)    Houston (1974)
                          Kress et al. (1982a);
                          Adams et al. (1988)
               3 h        7 to 56% (1)     Karnosky (1977);
               6 h        10 to 91 % (1)    Berrang et al. (1991)
 Cultivars = a variety of agricultural or horticultural crops produced by selective breeding or a vegetatively
 propagated tree selection; half-sib seedlings = seedlings with one parent in common; full-sib seedlings =
 seedlings in which both parents are in common; clones = vegetatively propagated individual genotypes;
 populations = seedlings derived from a common gene pool.
 Range of response is expressed as percentage of leaves showing visible symptoms (1); percentage of leaf area
 injured (2); or percentage from a leaf injury rating scheme (3).
December  1993
                                               5-45
                                   DRAFT-DO NOT QUOTE OR CITE

-------
 1     from any economic value related to growth (Tingey et al., 1990). Considerable genetic
 2     variation in O3 sensitivity has also been demonstrated for growth responses of crop plants
 3     (Table 5-2).  The range of responses displayed for visible foliar injury and growth, biomass
 4     or yield vary from species to species and from study to study.  However, it is not uncommon
 5     to have genotypes varying from no response to well over fifty percent leaf area injured or
 6     fifty percent growth or yield reductions in the same study.  Additional examples of genetic
 7     variation in O3 response are shown in Figure 5-7 for visible foliar injury and in Figure 5-8
 8     for growth. From Figure 5-7, we can see that depending on what population has been
 9     examined,  white ash (Fraxinus americana L.) and green ash (F. pennsylvanica Marsh.) could
10     have been classified as either O3 sensitive or O3  tolerant.  Also noticeable from this figure is
11     the large amount of variation in O3 tolerance of individual half-sib (one parent in common)
12     families from a given population.  From Figure 5-8, the heterogeneity within a given loblolly
13     pine (Pinus taeda L.) half-sib family in terms of growth is displayed.  This variability has
14     some interesting implications.  First, since plants of a  given species vary widely in their
15     response to O3 exposure, response relationships generated for a single genotype or small
16     group of genotypes may not adequately represent the responses of the species as a whole
17     (Temple, 1990).  Second, because of the genetic variability and  differential fitness existing
18     among different genotypes in a population of plants, O3  imposes a selective force favoring
19     tolerant genotypes over sensitive ones (Roose et al., 1982; Treshow,  1980).  Each of these
20     implications will be discussed in this section.
21
22     Mechanisms and Gene Numbers
23           Little is known about the genetic bases for O3 resistance mechanisms or about the
24     numbers of genes involved in these mechanisms  (Pitelka, 1988). Most O3 resistance
25     mechanisms involve a physiological cost  which will result in decreased growth and
26     productivity of resistant plants grown under O3 stress.  Partial or complete stomatal closure
27     in the presence of O3 is an example of a mechanism of resistance that has been demonstrated
28     for several plants (Engle and Gabelman,  1966; Thorne and Hanson, 1976; Reich, 1987;
29     Sumizono  and Inoue, 1986; Tingey and Taylor,  1982) and that involves a high physiological
30     cost as plants that have reduced  stomatal conductivity  will also have reduced carbon
31     assimilation for growth (Ehleringer, 1991).  Tolerance of internal leaf tissues to O3 may

       December 1993                           5-46       DRAFT-DO NOT QUOTE OR CITE

-------
    TABLE 5-2. EXAMPLES OF INTRASPECIFIC VARIATION IN GROWTH
              RESPONSES FOLLOWING OZONE EXPOSURES
Species
Crops and
Non-Woody
Plants
Agrostis capillaris L.
(Bentgrass)
Begonia semperflorens
Hort. (Bedding
begonia)
Festuca arundinacea
Schreb. (Fescue)
Lycopersicon
esculentwn L.
(Tomato)
Phaseolus vulgaris L.
(Snapbean)
Plantago major L.
(Common plantago)
Raphanns sativus L.
(Radish)
Silene cucahalus
(Bladder campion)
Solatium tuber o sum L.
(Potato)

Spinacia oleracea L.
(Spinach)
Trees and Other
Woody Plants
Acer rubrum L.
(Red maple)
Abies alba Mill.
(Silver fir)
Pinus elliottii
Engelm. (Slash pine)
Genetic
Unit"



Populations
Cultivars
Cultivars
Cultivars
Cultivars
Populations
Within
Cultivar
Populations
Cultivars

Cultivars


Populations
Populations
Half-sib
families
Concentration



60 ppb
500 ppb-
4 h/day
250 ppb-
4 h/day
400 ppb-
6 h/day
400 ppb
1.5 x ambient
60 ppb-
7h
72 ppb-
7 h
80 ppb-
7 h/day
70 nl/
1-7 h/day
.1 n\l
1-4 h/day -
3 days/week
35 ppb-
12 h/day
150ppb-
6 h/day

130 ppb -
7 h/day


750 ppb -
7 h/day
250 ppb -
7 h/day
3 x ambient
Duration



4 weeks
2 days
4 days
7 days
2h
1 growing
season
mean-
44 days
mean-
54 days
42 days
2 weeks
3 weeks
4 weeks
8 days

38 days


3 days
10 days
3 growing
seasons
Range of
Response



-45 to
+20%(2)
-59 to 0%(2)
-16 to
+ 10% (2)
-53 to -35% (2)
-50 to -4% (2)
-54 to -17%(3)
-26 to -2% (3)
-73 to -44% (3)
-68 to -50% (3)
-24 to 0%(1)
-40 to -5%(2)
-75 to -48% (2)
-10 to 0%(2)
-40 to 0%(2)

-56 to -28% (2)


-36 to -17%(1)
-18 to +3%(1)
-20 to 0%(1)
Reference



Dueck et al.
(1987,)
Reinert and
Nelson (1979);
Reinert and
Nelson (1980)
Flagler and
Younger (1982)
Reinert and
Henderson (1980);
Temple (1990)
Heck et al. (1988);
Temple (1991);
Eason and Reinert
(1991)
Reiling and
Davison (1992a)
Gillespie and
Winner (1989)
Ernst et al. (1985)
Pell and Pearson
(1984);
Ormrod et al.
(1971)
Heagle et al.
(1979)


Townsend and
Dochinger (1974)
Larsen et al.
(1990)
Dean and Johnson
(1992)
December 1993
                              5-47     DRAFT-DO NOT QUOTE OR CITE

-------
        TABLE 5-2 (cont'd).  EXAMPLES OF EVTRASPECIFIC VARIATION IN GROWTH
                         RESPONSES FOLLOWING OZONE EXPOSURES
Species
Pinus taeda L.
(Loblolly pine)


Pinus taeda L.
(Loblolly pine)



Populus tremuloides
Michx. (Trembling
aspen)
Rhododendron
obtusum
(Lindl) Planch.
(Azalea)
Genetic
Unit"
Full-sib
families


Half-sib
families



Clones
Ambient

Cultivars



Concentration
50 ppb-
6 h/day
1.9 x ambient

Ambient -t-
60 ppb
2.5 x ambient
250 ppb

26.4 ppm-h
3 growing seasons

250 ppb-
3 h/day


Duration
28 days
2 growing
seasons

1 growing
season
1 growing
season
8h
92 days
-24 to -
12%(2)
6 days



Range of
Response
-18toO%(l)
-19 to 0%(2)


-27.5 to
+3%(2)
-19 to -2%(2)
-22 to
+30%(2)
-74 to -5% (2)


-43% to 0(2)



Reference
Kress et al.
(1982b);
Shafer and Heagle
(1989)
Adams et al.
(1988);
Qui et al. (1992);
Winner et al.
(1987)
Karnosky et al.
(1992);
Wang et al. (1986)
Sanders and
Reinert (1982)


       aCultivars = a variety of agricultural or horticultural crops produced by selective breeding or a vegetatively
       propagated tree selection; half-sib seedlings = seedlings with one parent in common; full-sib seedlings =
       seedlings in which both parents are in common; clones = vegetatively propagated individual genotypes;
       populations = seedlings derived from a common gene pool.
       Range of response is expressed as decrease compared to charcoal-filtered-air control plants in terms of growth
       (1), biomass (2) or yield (3).
 1      involve the production of antioxidant defense compounds (Lee and Bennett, 1982; Gupta
 2      et al.,  1991) or other types of biochemical defense systems.  The extent to which these
 3      internal tolerance mechanisms have physiological costs associated with them is not yet
 4      understood, but it is likely that increased defense compound production, triggered by O3, will
 5      impact the amount of carbon available for growth (Ehleringer, 1991).  The genetic regulation
 6      of these or other O3 resistance mechanisms has not yet been thoroughly characterized.
 7           Whether or not O3 resistance is due to single gene or multi-gene control will affect the
 8      rate and the extent of resistance development (Roose,  1991).  Rapid stomatal closing in the
 9     presence of O3 appears to be under the control of either a single gene or a few genes in
10     onion (Allium cepa L.) (Engle and Gabelman,  1966),  some bean (Phaseolus vulgaris L.)
11      cultivars (cultivated varieties) (Knudson-Butler and Tibbitts, 1979), soybean (Glycine max L.)
12     (Damicone and Manning,  1987) and petunia (Petunia  spp.) (Elkiey and Ormrod, 1979).
       December 1993
5-48
DRAFT-DO NOT QUOTE OR CITE

-------
       250-
                        A.   F. americana
                                 4567
                                  Provenance
                                                     9   10
250


200

150
    .5, 100-
501

 0

                               B.   F. pennslvanica
                        111
                                III
               12345
                          6  7   89  10  11 12  13 14  15  16
                           Provenance
Figure 5-7.  The average injury index for visible foliar injury after exposure of
           1-year-old seedlings to 50 pphm O3 for 7.5 h. Each mean shown represents
           the average of five trees per family. There were either four or five half-sib
           families for each white ash (Fraxinus americana L.) provenance (geographic
           location) and either three or four families for each green ash
           (F. pennsylvanica Marsh.) provenance.  The specifics of the experimental
           design are reported in Karnosky and Steiner (1981).
December 1993
                             5-49
                                     DRAFT-DO NOT QUOTE OR CITE

-------
                   113 137 163  188 213 237  263  288  313  337  363  388  413  437  463  488  513
                                       Midpoint of Biomass Class (g)

       Figure 5-8.  Frequency distribution showing the variability hi O3 response (midpoint of
                   whole-plant biomass) within one half-sib family of loblolly pine (P. taeda L.)
                   exposed to increasing levels of O3 under chronic-level field conditions over
                   several growing seasons (Adams  et al., 1988).  The arrows show the mean
                   response for each of the three O3 treatments (sub-ambient, ambient and
                   above-ambient O3). The specifics of the experimental design are reported
                   by Adams et al. (1988). This figure was developed by Taylor (1993).
 1     Generally, resistance mechanisms appear to be more complex (Karnosky, 1989a) and seem to
 2     involve multiple gene control as has been demonstrated in tobacco (Nicotiana tabacum L.)
 3     (Aycock, 1972; Huang et al., 1975, Povilaitis, 1967), some bean cultivars (Mebrahtu et al.,
 4     1990a,b,c), corn (Zea maize L.)  (Cameron, 1975), tall fescue (Festuca arundinacea Schreb.)
 5     (Johnston et al., 1983), potato (Solatium tuberosum L.) (DeVos et al., 1982; Dragoescu
 6     et al., 1987) and loblolly pine (Pinus taeda L.) (Weir, 1977; Taylor, 1993).
 7
 8     Genetic Implications of Ozone Effects:  Managed Ecosystems
 9          Because of the high cost involved in conducting long-term growth studies to determine
10     O3 effects on  plants, only a small proportion of the total number of commercial crop
11     cultivars and of the important tree seed sources, families, clones and cultivars have been

       December 1993                          5-50      DRAFT-DO NOT QUOTE OR CITE

-------
 1     adequately examined for O3 sensitivity.  Still, a tremendous amount of variation has been
 2     found, as  was described previously in the first O3 criteria document (U.S. Environmental
 3     Protection Agency, 1986) and in Tables 5-1 and 5-2 of this section.
 4          Plant breeders and nurserymen working in locations with high O3 concentrations have
 5     inadvertently developed selections more tolerant to O3 than those developed in locations with
 6     low O3 exposures  (Reinert  et al., 1982, Roose et al., 1982).  "Team" alfalfa (Medicago
 1     sativd) and "Kennebec", "Pungo" and "Katahdin" potato were developed at the USDA
 8     Research  Center at Beltsville, Maryland where 0.120 ppm O3 is commonly exceeded (Lefohn
 9     and Pinkerton, 1988; Ludwig and Shelar, 1980).  These cultivars have proven to be more
10     O3 tolerant than cultivars developed elsewhere (Reinert et al., 1982).  Similarly, cotton
11     (Gossypium spp.) and sugar beet (Phaseolus spp.) cultivars developed in southern California,
12     where O3 levels are among the highest in the county, are more O3  tolerant than cultivars
13     developed in low O3 areas  (Reinert et al.,  1982).
14          Nurserymen, Christmas tree growers and seed orchard managers have all routinely
15     discarded pollution-sensitive chlorotic dwarf and tipburned white pine trees because of their
16     slow growth in areas with high O3 exposures (Umbach and Davis,  1984). Thus, they have
17     contributed to the  selection of more O3-tolerant commercial forests.
18          While these examples suggest that selection of O3-tolerant genotypes is possible, this
19     topic remains a highly debatable issue, and the general consensus of the scientific community
20     is that top priority should be given to solving pollution problems at their source (Karnosky
21     et al., 1989b) and not in selecting pollution-tolerant cultivars.
22           An interesting set of experiments by Barnes et al. (1990) and Velissariou et al. (1992)
23     have described a concern about the modern crop varieties that have been developed in clean-
24     air environments,  but that are being routinely grown in areas with  elevated O3 exposures.
25     These authors speculated that breeders of spring wheat (Triticum aestivwn L.) grown in
26     Greece had inadvertently selected varieties with increased O3 sensitivity due to their higher
27     rates of stomatal conductivity (Velissariou et al., 1992). Vellisariou et al. (1992) found  a
28     significant correlation between year of introduction and stomatal conductance with stomatal
29     conductance increasing with the more modern introductions.  The authors suggested that the
30     selection for higher yields had resulted in a higher O3 uptake for the modern spring wheat
31     cultivars, contributing to their increased O3 sensitivity.  When they compared the relative

       December 1993                           5.5!       DRAFT-DO NOT QUOTE OR CITE

-------
 1      growth rates of spring wheat cultivars released over the period from 1932 to 1980, the
 2      modem cultivars had more foliar injury and more growth decrease when grown in the
 3      presence  of O3  (Barnes et al., 1990; Velissariou et al., 1992).
 4
 5      Genetic Implications of Ozone Effects:  Natural Ecosystems and Biodiversity
 6           Air pollutants can affect the genetics of plant populations in two ways: They may
 7      increase mutation rates or they may apply selection pressures which may eventually lead to
 8      adaptive  responses (Cook and Wood, 1976). The issue of O3-induced changes in mutation
 9      rate has not been adequately studied yet, but recent evidence by Floyd (1992) suggests that
10      DNA may be affected by O3 to induce mutation in plants.  However, there is evidence that
11      O3 may be affecting plant populations via natural selection.  According to Bradshaw and
12      McNeilly (1991), there are three stages of selection-driven population change:   Stage I.
13      Elimination of the most sensitive genotypes; Stage n:  Elimination of all genotypes except
14     the most resistant; Stage HI:  Interbreeding of the survivors.
15          The first report of O3 as a selective force in plant populations was that involving lupine
16     (Lupinus bicolof) populations in the greater Los Angeles area (Dunn,  1959).  Local
17     Los Angeles area populations were more O3 resistant than populations originating from
18     cleaner-air areas.  Berrang et al. (1986, 1989, 1991) have presented evidence for population
19     change in trembling aspen (Populus tremuloides L.). Aspen clones from across the United
20     States were sampled randomly from populations in polluted and non-polluted areas. Aspen
21     from areas with high ambient O3 concentrations were visibly injured to a lesser extent by
22     experimental O3 exposures than clones from areas with low O3 concentrations (Berrang
23     et al., 1986,  1991).  Similar results were seen for field trials of O3 injury (Berrang et al.,
24      1989). More recently,  growth rate and biomass differences have been reported for aspen
25     clones differing in O3 tolerance (Karnosky et al., 1992).  Berrang et al. (1989) suggest that
26      sensitive genotypes are not killed directly by O3, but are eliminated through intraspecific
27      competition for light, nutrients and water with their resistant neighbors.  Spatial (population)
28      variation in O3 resistance that is related to background O3 pollution has also been
 29      demonstrated in British populations of plantago (Plantago major L.) (Reiling and Davison,
 30      1992a,b).
        December 1993                           5-52       DRAFT-DO NOT QUOTE OR CITE

-------
 1          There have been three concerns raised regarding the spatial variation studies of
 2     O3 resistance.  First, since O3 does not generally show steep concentration gradients, spatial
 3     studies must  involve populations that are great distances from one another so that it is
 4     difficult to determine whether geographical differences in O3 resistance are primarily related
 5     to local O3 exposures or to other environmental factors (Reiling and Davison, 1992a).
 6     Second, spatial studies are limited by the general absence of historical records of ambient
 7     O3 concentrations at the sites where the populations were sampled (Bell et al., 1991).  Third,
 8     no O3 study has collected plants from the same population over time to demonstrate
 9     O3-induced population change over time (Bell et al., 1991) as has been demonstrated for
10     other pollutants. However,  Karnosky (1981b; 1989b) studied the O3  symptom expression
11     and survival of over 1,500 eastern  white pine trees growing in southern Wisconsin and found
12     that O3-sensitive genotypes had a ten-times-higher rate of mortality than did the O3-resistant
13     genotypes over a 15-year study (Table 5-3).  This is direct evidence of Stage I of natural
14     selection occurring.  Further evidence of this  type was presented by Heagle et al. (1991) who
15     found a population change in O3 sensitivity over two years with white clover (Trifolium
16     repens L.) exposed to O3 in open-top chambers.  A high O3 dose at the end of the study
17     caused significantly less foliar injury in plants which survived two seasons of exposure to
18     high O3 concentrations than on plants that had survived low O3 concentrations.
19
20
            TABLE 5-3.  MORTALITY OF THREE OZONE SENSITIVITY CLASSES OF
           EASTERN WHITE PINE  (PINUS STROBUS L.) TREES DURING THE PERIOD
                                        FROM 1971 TO 1986
Sensitivty Class11
Resistant
Intermediate
Sensitive
Number Trees
1386
98
57
Number Trees Dead
34
3
14
Percent Mortality
2.4%
3.1%
24.6%
       ^Resistant = Not showing visible foliar injury during the study; Intermediate = Showing visible injury,
        including foliar tipburn during one or two years; Sensitive = Showing visible injury, including foliar tipburn,
        short needles and poor needle retention for three or more years of the study.
       Source: From Karnosky, (1989b).
       December 1993                           5.53       DRAFT-DO NOT QUOTE OR CITE

-------
 1           The rate of evolution is dependent on: (1)  the selection pressure; (2) the magnitude of
 2      the genetically controlled variability; and, (3) the number of genes involved (Roose, 1991).
 3      Long-lived species, such as trees, will evolve more slowly than annuals or biennials (Barrett
 4      and Bush, 1991).  Gillespie and Winner (1989) found O3 to be a strong and rapid selective
 5      force with radish.  Ozone resistance was expressed within one generation following a series
 6      of artificial pollinations with  various populations from the cultivar "Cherry Belle".
 7           Whether or not the loss of some genotypes from plant populations is important is a
 8      debatable question. However,  it is likely that sensitive genotypes are being lost from natural
 9      ecosystems with current O3 exposures. Field  studies documenting differential growth rates
10     of O3-sensitive and tolerant genotypes of eastern white pine in natural ecosystems influenced
11      by O3 were summarized in the original air quality criteria document for O3 (U.S.
12     Environmental Protection Agency,  1986).  Similar findings have subsequently been reported
13     for O3-sensitive and tolerant Jeffry pine (Pinus Jeffrey, Grev.  and Balf.) trees in California
14     (Peterson et al.,  1987).  It is likely that these growth rate differences affect the competitive
15     ability of O3-sensitive genotypes and increase their mortality rate (Karnosky, 1989b).
16           While some loss of rare alleles (one of a series of genes that are alternative in
17     inheritance) and change in gene frequency is likely with loss of sensitive genotypes, the
18      significance of these effects  on biodiversity is unknown (Barrett  and Bush, 1991). If the
 19      remaining population of O3-resistant plants is less adaptable to subsequent change due to a
20      reduced redundancy, as has  been predicted by Gregorius (1989), or if O3 sensitivity is linked
 21      to other traits such as rapid  growth or high productivity, as has  been suggested because of
 22      the inherently higher gas exchange rates of some O3-sensitive genotypes (Barnes  et al., 1990;
 23      Thorne and Hanson, 1976; Turner et al., 1972; Velissarious  et al., 1992), then losing these
 24      sensitive genotypes is both biologically and economically important.  This remains a point  of
 25      scientific debate. While the evolution of resistance to air pollution is hypothesized to
 26     contribute to the loss of genetic variability (Scholz et al., 1989; Karnosky, 1991), other
 27     scientists suggest that there  is little experimental evidence for concluding that genetic
 28     diversity is actually threatened by air pollution and that air pollution has less important
 29     implications for plant populations than do factors such as global climate change and habitat
 30     fragmentation (Parson and Pitelka, 1991; Taylor and Pitelka, 1991).  Clearly, there is a need
 31     for additional research in this area of O3 effects in plant biodiversity (Karnosky et al., 1989).

         December 1993                            5-54       DRAFT-DO NOT QUOTE OR CITE

-------
 1      Reproductive Aspects and Related Genetic Implications
 2           In the previous discussion in this section, only natural selection at the whole-plant level
 3      has been mentioned.  This type of selection occurs as plants compete with their neighbors for
 4      survival and the ability to reproduce.  Selection is thought to also occur during the
 5      reproductive process (Feder and Sullivan, 1969; Krause et al., 1975) and this is referred to
 6      as gametophytic selection (Mulcahey, 1979; Wolters and Martens, 1987) or fertility selection
 7      (Venne et al., 1989). The ability of gametophyte (haploid part of the plant-life cycle)
 8      selection to modify the sporophytic generation depends on two critical issues:  pollen genes
 9      should be expressed after meiosis (cell divisions leading to production of gametes) and those
10      same genes should also be expressed in the sporophytes (diploid part of the plant-life cycle)
11      (Mulcahey and Mulcahey, 1983). This genetic overlap has been demonstrated in  some
12      species (Mulcahey, 1979; Searcy and Mulcahey, 1985; Walsh and Charlesworth,  1992).
13      Indirect evidence for O3-induced gametic selection was presented for Scot's pine (Pinus
14     sylvestris L.) by Venne et al. (1989). Based  on their studies of the effects of O3 on the
15      pollen germination and tube elongation of some thirty Scots pine clones, they found that
16     O3 could markedly change the relative male contribution to successful fertilization.
17     However, this study did  not actually examine offspring as would be needed to positively
18     prove O3-induced gametophytic  selection.
19          Studies of O3 effects on pollen germination and tube elongation have generally found a
20     negative impact of O3 on this critical element of reproduction (Table 5-4). Whether or not
21      selection is occurring at the pollen level  because of a selective disadvantage of the pollen
22     from sensitive genotypes is a debatable issue. Feder (1986) and Krause et al.  (1975) found
23     that the pollen from O3-sensitive genotypes of petunia and tomato (Lycopersicon esculentum
24     L.) was more severely affected by O3 than pollen from tolerant genotypes, suggesting that
25     gametophytic selection could be occurring. Similar results were found for Scots pine clones
26     by Venne et al.  (1989).  These authors found that the relative male contribution for charcoal-
27     filtered air versus O3-treated conditions was very different and could potentially lead to a
28     strong gametophytic selection response caused by O3.  However, Hanson  and  Addis (1975)
29     did not see any differences in the effect of O3 on the pollen from sensitive and tolerant
30     petunia genotypes, and Benoit et al.  (1983) found no apparent differences in the susceptibility
        December 1993                           5.55       DRAFT-DO NOT QUOTE OR CITE

-------
         TABLE 5-4.   EXAMPLES OF OZONE EFFECTS ON POLLEN GERMINATION
                                   AND TUBE ELONGATION
Species
Nicotiana tobacum L.
(Tobacco)
Petunia hybrida
(Petunia)
Pinus strobus L.
(Eastern white pine)
Zea mays L.
iCorn)
Pollen
Germination
Decrease
Not tested
No effect
Decrease
Pollen Tube
Elongation
Decrease
Decrease
Decrease
Not tested
Reference
Feder, 1968;
Feder and Shrier, 1990
Feder and Shrier, 1990
Benoitetal. 1983
Mumfordetal. 1972
 1      of eastern white pine pollen from O3-sensitive or tolerant genotypes.  Clearly, the question of
 2      whether O3-induced gametophytic selection is occurring has not yet been resolved.
 3           Reduced flowering as the result of prolonged fumigation with O3 has been shown in
 4      Bladder campion (Silene cucubalus) (Ernst et al.,  1985). Decreased floral initiation and
 5      decreased floral productivity under long-term O3 exposures have also been reported in
 6      geranium (Pelargonium spp.) and carnation (Dianthus caryophyllus)  (Feder, 1970).
 7      Ozone-induced impairment of flowering will reduce the fitness of the affected genotypes,
 8      populations or species and may result in the eventual loss of these genetic units from the
 9      O3-stressed ecosystem.  Reduced eastern white pine fecundity in air pollution-stressed
10      ecosystems has been reported by Houston and Dochinger (1977).
11
12      Genetic Summary
13           Plant species, cultivars, populations  and individuals within populations display variable
14      responses to O3. Variability in O3 responses between and within species was described in
15      the previous O3 criteria document (U.S. Environmental Protection Agency, 1986).
16      An important component of this variation is genetically controlled. The specific genes
17      controlling O3 response and involved in mechanisms of O3 tolerance are  as yet largely
18      unknown.  However, control of stomatal conductance and internal biochemical defense
19     systems are among the most commonly described tolerance mechanisms.  Ozone tolerance is
20     generally thought to be controlled by multiple genes.
       December 1993
5-56
DRAFT-DO NOT QUOTE OR CITE

-------
 1          There are implications of genetic variation in O3 response, both for managed and
 2     natural ecosystems.  These are summarized below along with the relative degree of
 3     uncertainty attached to each.
 4          It is known, with a great deal of certainty, that plants have a high degree of genetic
 5     variation in O3 response.  Thus, exposure-response equations and yield-loss equations
 6     developed for a single or small number of cultivars, genotypes, families or populations may
 7     not adequately represent the response of thespecies as a whole.  As a corollary to this,
 8     sensitive responder genotypes will not be protected by air-quality standards based on mean
 9     responses.
10          The issue of O3 effects on biodiversity via natural selection is a topic of debate within
11     the scientific community.  The potential for natural selection for O3 tolerance and associated
12     loss of sensitive genotypes is regional in nature, unlike well known, point-source pollution
13     impacts which occur on local plant populations.  However, the intensity of O3 selection is
14     generally thought to  be  quite low, 0.3 or less (Taylor and Pitelka, 1992), in the majority of
15     the United States.  The extent that germplasm has been or is continuing to be affected in
16     terms of allele loss or gene frequency changes by O3 and how this might be impacting the
17     genetic adaptability of populations is an open and important research question.
18          While it is well known that individual plants within a species vary in their O3 tolerance,
19     the physiological costs to tolerant plants are not known in terms of carbon assimilation and
20     allocation. Tolerance mechanisms based on reduced stomatal conductivity in the presence of
21     O3 would likely reduce growth of tolerant plants. Similarly,  tolerance mechanisms based on
22     the productivity of antioxidant compounds will likely shunt plant resources away from growth
23     to the production of the defense compounds.  The characterization of the extent and types of
24     physiological costs involved in O3 tolerance remains an important research question.
25
26     5.4.3   Environmental Biological Factors
27          The previous criteria document (U.S. Environmental Protection Agency,  1986)
28     discussed pollutant-plant-pest and pollutant-plant-pathogen interactions together, and provided
29     a tabular summary of pathogen effects.  However, in light of the numerous studies of insect
30     and pathogen interactions that have appeared in recent years,  the topics are dealt with
       December 1993                           5,57       DRAFT-DO NOT QUOTE OR CITE

-------
 1     separately below.  Nevertheless, it is worth reiterating several points made in the previous
 2     criteria document:
 3            • pests and diseases are natural components of managed and natural
 4              ecosystems;
 5
 6            • significant crop and timber losses result from pests and pathogens;
 7
 8            • the establishment of disease and pest infestations and their subsequent
 9              development involve complex interactions between host plant, the
10              environment and the causal organism;
11
12            • the generalized disease (or pest infestation)  cycle involves the arrival of the
13              pathogen or pest on the host plant surface or its introduction into the host
14              plant tissues through wounds or as a result  of insect feeding activity;
15
16            • growth and development or propagation of  the pathogen or pest only occurs
17              if all environmental conditions are  favorable;
18
19            •  such development leads to various  degrees of host tissue destruction or
20               malfunction, and usually culminates in the causal organism entering a
21               reproductive stage and producing propagules (e.g., spores or eggs) that
22               facilitate its spread.
23
24           Ozone may modify any stage of the disease cycle directly, by affecting the causal
25      organism itself, or indirectly by effects on the host plant (Lechowiez, 1987).  Conversely,
26      the plant-pest interaction may modify the sensitivity of the host plant to O3.
27           The roots of many members of the pea family (including many  important crops such as
28      soybeans, beans and peas) are infected by  symbiotic nitrogen-fixing bacteria (Rhizobium spp.)
29      leading to the formation of bacteria-rich nodules that contribute to the nitrogen economy of
30      the plant, through their ability to fix and convert atmospheric nitrogen, N2, to biologically
31      useful forms.  Other nitrogen-fixing microorganisms  are associated with the roots of several
32      species, and in many cases roots are invaded by species of soil fungi to form mycorrhizal
33      symbioses that assist in  root functioning. These symbioses constitute micro-ecosystems and
34      are discussed more fully in Section 5.7 as they relate to forest tree species.
35           Biological interactions also affect the growth of plants in populations (pure stands) and
 36      communities (mixtures of species) through the individual plants' competition for available
 37      resources (light, CO2, water, nutrients).  Such plant-plant interactions are features of all
 38      managed and natural ecosystems, but  they operate at the indivdual plant level. Hence the
        December 1993                           5.53       DRAFT-DO NOT QUOTE OR CITE

-------
 1     effects of oxidants on these interactions are discussed in both the present section and in
 2     Section 5.7 which deals will ecosystem responses.
 3
 4     5.4.3.1   Oxidant-Plant-Insect Interactions
 5          The previous criteria document (U.S. Environmental Protection Agency,  1986),
 6     concluded that little was known at that time about O3-insect interactions.  Since then the
 7     topic has been covered in several reviews:  Fluckiger et al. (1988), Hughes (1988), Manning
 8     and Keane (1988), and Hain (1987). Relevant studies of the effects of O3 on the feeding
 9     preference of herbivorous insects, and on their growth, fecundity, and survival are presented
10     in Table 5-5.  As can be readily seen in this summary, the information is widely scattered
11     among a wide range of host plants and pests. Nevertheless, there appears to be a general
12     trend in the observations suggesting that O3-induced changes in the host plants frequently
13     result in increased feeding preference of a range of insect species, although this may or may
14     not be reflected  in effects on the growth of the insect.
15          However,  in most studies, the effects have been far from clear-cut.  For example,
16     variable responses were observed with the aphid, Aphis fabae, on broad bean (Brown et al.,
17     1992), with the  aphids, Acyrthosiphon pisum and Aphis rumicis, on pea and dock,
18     respectively, and the beetle, Gastrophysa viridula on dock (Whittaker et al., 1989), with  the
19     Mexican bean beetle, Epilachna varivestis, on Corsoy soybean (Endress and Post,  1984), and
20     with the gypsy moth, Lymantria dispar, on white oak (Jeffords and Endress, 1984).
21     Although statistically significant effects were frequently observed, they did not provide any
22     consistent pattern of insect growth response to different levels or patterns of exposure.
23          Brown  et al. (1992) observed that the response of Aphis fabae depended  upon the
24     dynamics of exposure:  growth was stimulated in short-term (< 24 h) continuous exposures
25     or in episodic exposures over several days, whereas longer continuous exposures caused
26     decreased growth.  Chappelka et  al. (1988c) found that O3 consistently enhanced the feeding
27     preference and larval growth of the Mexican bean beetle on soybean, leading to increased
28     defoliation.  Although the cultivar Forrest was significantly more sensitive to O3 than Essex,
29     this difference did not lead to any differences in insect behavior and  development.  Similarly,
30     clear stimulatory responses were  observed with pinworm, Keiferia lycopersicella, on tomato
31     (Trumble et al., 1987), with an aphid,  Phyllaphis fagi, and a weevil, Rhynchaenus fagi, on

       December 1993                            5.59       DRAFT-DO NOT QUOTE OR CITE

-------
                                           TABLE 5-5.  OZONE EFFECTS  ON INSECT PESTS
I
cr
Host Plant Inse< i
CROP SPECIES
Broad bean aphid
Pea/aphid
Kidney bean/ aphid
Soybean/beetle
(cv Corsoy)
Exposure*1

3 day, 0.085 ppm
< 24 h, 0. 1 ppm
> 24 h, 0. 1 ppm
8 h/day, episodic
4-8 day, var.
14 day, var.
16 day, var.
21 day, 7 h/day, var.
Experimental Conditions

chamber, whole plant
chamber, whole plant
chamber, whole plant
chamber, whole plant
chamber, whole plant
OTC
chamber
OTC
Effect of Ozone on Insect

3-13% decreased growth rate
17% increased growth rate
12% decreased growth rate 15%
increased growth rate
variable effects on growth
15-50% reduction in growth of
insect
variable feeding preference
0.11>0.0>0.05> 0.03 ppm
Reference

Dohmen (1988)
Brown et al. (1992)
Whittaker et al. (1989)
Braun and Fluckiger (1989)
Endress and Post (1985)
Chappelka et al. (1988c)
       (cvs Essex. Forrest)
     Tomato/pinworm
     NATURAL
     VEGETATION

     Milkweed/monarch
      butterfly

     Dock/aphid

     Dock/beetle


     TREES SPECIES

     European beech/aphid
2-4 day, 3 h/day,
0.28 ppm
chamber, detached leaf
chamber, whole plant
17-19 day, 7 h/day
0.150-0.178 ppm

15 day, var.

15 day, var.
2 mo., var.
chamber, whole plant


chamber, whole plant

chamber, whole plant
OTC
 feeding preference increased and
 greater larval growth

 80% in crease in larval
 development; no effect on
 fecundity
no feeding preference but greater
larval growth rate

10% increased growth rate

10% larger egg batches; 4-fold
greater larval survival
75 % increase in number
Trumble et al. (1987)
Bolsinger et al. (1992)


Whittaker et al. (1989)

Whittaker et al. (1989)
Braun and Fluckiger (1989)

-------
                                        TABLE 5-5 (cont'd). OZONE EFFECTS ON INSECT PESTS
3     Host Plant/Insect
cr  	
                                     Exposure
                                                Experimental Conditions
    Effect of Ozone on Insect
           Reference
 n>
       TREE SPECIES
       (cont'd)
       European beech/weevil    72 h, var.
       Cottonwood/beetle
                        5 h, 0.2 ppm
       Ponderosa pine/bark      natural
        beetle
                                                OTC
                                                       OTC
                                                none, field


White oak/gypsy moth     11 day, 7 h/day. var.      chamber, leaf disks
2-fold increase in feeding
preference

22-60 % greater consumption of
foliage, but decreased fecundity

increased infestation but in
decreased survival

variable feeding preference
0.15 > 0.03 > 0.09 ppm
Hiltbrunner and Fluckiger (1992)


Jones and Coleman (1988)
Coleman and Jones (1988)

Hain (1987)


Jeffords and Endress (1984)
      "var." indicates a range of exposures.
     b
       "chamber" indicates closed chamber; OTC indicates open-top field chamber.
1
8
O

-------
 1      European beech (Braun and Fluckiger,  1989; Hiltbrunner and Fluckiger, 1992), with the
 2      monarch butterfly, Danaus plexippus, on milkweed (Bolsinger et al., 1992), and with
 3      infestation by the willow leaf beetle, Plagiodera versicolora, on cottonwood (Coleman and
 4      Jones, 1988).  However, there was  less egg-laying by Plagiodera on O^-treated foliage, and
 5      treatment had no effect on beetle growth rates  and survival (Jones and Coleman, 1988).
 6           In view of previous experiments in which it was clearly demonstrated that aphid growth
 7      was significantly stimulated by ambient pollutant mixtures containing 63, SO2, and NO2, and
 8      in light of other reports of O3-induced  stimulations of insect growth, the inhibitory effects of
 9      O3 on the growth of Aphis fabae on Broad Bean (dohmen, 1988), Or Kidney bean (Braun
10      and Fluckiger,  1989), may be anomalous.  The inhibitory effects on broad bean were only
11      observed at low 03 levels: exposure to higher concentrations resulted in a stimulation of
12      aphid growth, which Dohmen (1988) attributed to the increased rate of leaf senescence of the
13      host plant.  The effects observed on kidney bean could not be accounted for by differences  in
14     the amino acid composition of the plant sap, although differences in other constituents or
15     direct effects of O3 on the pea aphid itself could not be ruled out (Braun and Fluckiger,
16     1988).
17           A well-established indirect stimulatory effect is the predisposition to bark beetle attack
18     of ponderosa pine injured by exposure to O3.  However, the infested trees do not favor good
19     brood production; O3 injury results in  a more susceptible but less suitable host (Hain, 1987).
20           In all of these studies, the focus was on  direct or indirect effects of 03 on the insect.
21     With the exception of the work of Braun and  Fluckiger (1988), any effects on the host plant
22     that were reported were confined to observations on visible symptoms of foliar injury.  The
23     only report of an  O3-insect interaction affecting the response of the host plant appears to be
24     that of Rosen and Runeckles (1976). This study showed that exposure to sub-acute levels of
25      O3 and infestation with the greenhouse whitefly, Trialeurodes vaporarionm, acted
26      synergistically (i.e., more than additively) in causing leaf injury and accelerated senescence
27      of kidney bean.  However,  the extent  to which other insects with sucking mouthparts, such
28      as aphids. might be involved in similar interactive responses is unknown, as is the nature of
 29      any interactions which involve pests that ultimately invade and develop within the host plant,
 30      such as those that cause the  formation of galls.
        December 1993                           5-62       DRAFT-DO NOT QUOTE OR CITE

-------
 1           The reports of O3-insect-plant interactions are thus scattered among a wide range of
 2      host plant and insect species, and only represent a minute fraction of the plant-insect
 3      interactions that involve crop and native species.  Although there appears to be a trend in the
 4      limited data available that suggests that exposures to moderate O3 levels may increase the
 5      likelihood of insect attack and its consequences,  there is insufficient information to decide
 6      whether extrapolation of this generalization is warranted or not.  Even if the generalization is
 7      valid, it is not possible to generate any quantitative measure of response.  Before such
 8      estimates will be possible on a broad scale, studies of a much wider range of plant insect-
 9      systems will be needed, together with systematic, in-depth studies of individual systems,
10     aimed at determining the long-term effects on both the host plant and the insect. Such
11      studies should include investigations of biological control systems employing beneficial
12     insects which are increasing in use as alternatives to chemical insecticides and herbicides.
13
14     5.4.3.2  Oxidant-Plant-Pathogen Interactions
15          Plant disease is the result of infection by fungi, bacteria, mycoplasmas, viruses and
16     nematodes.  Recent reviews of pathogen-plant-O3 interactions have been published by
17     Dowding (1988) and Manning and Keane (1988), and extend the coverage of the previous
18     criteria document (U.S. Environmental Protection Agency, 1986) in which the results of
19     published studies of the effects of O3 on disease development were summarized in tabular
20     form.  Interactions involving fungal pathogens occupied most of that review, and more recent
21     studies have maintained this emphasis.
22          The previous criteria document concluded  that it was "impossible to generalize and
23     predict effects in particular situations." (U.S. Environmental Protection Agency, 1986;).
24     However, Dowding (1988) has since concluded  that pathogens which can benefit from
25     injured host cells or from disordered transport mechanisms are enhanced by pollution insult
26     to their hosts, whereas those that require a healthy mature host for successful invasion and
27     development are depressed by pollutant stress to their host.
28          This conclusion is supported by evidence that the development of diseases caused by
29     obligate parasites such as the rust fungi and bacterial pathogens  is usually reduced by
30     O3. As shown by the observations summarized in Table 5-6, reductions in disease
31     development were observed in five of the nine studies of obligate fungal parasites listed

       December 1993                           5_63       DRAFT-DO NOT QUOTE OR CITE

-------
TABLE 5-6.  OZONE-PLANT-PATHOGEN INTERACTIONS
«
o>
1
1




t

!
8
|
i
Host Plant
OBLIGATE FUNGI
Kidney bean
Barley
Cottonwood
Lilac
Oats
Wheat


FACULTATIVE FUNGI
Barley
Cabbage

Pathogen

Uromyces phaseoli
Erysiphe graminis
Melampsora medusae
Microsphaera alni
Puccinia coronata
Erysiphe graminis
Puccinia graminis
Puccinia graminis
Puccinia recondita
Drechslera teres
Gerlachia nivatis
Helminthosporium
sativum
Fusarium oxysporum

Effect of 03 on Disease

increased number of
smaller pustules
reduced infection but
greater spore production
reduced infection and
development
no effect
reduced infection and
development
increased infection and
development
reduced infection and
development
reduced development
reduced infection and
development
increased infection
increased infection
no effect
decreased development

Effect of Disease on 03 Response

reduced injury on severely
diseased leaves
not reported
not reported
not reported
no effect
not reported
reduced leaf injury
no,t reported
not reported
not reported
not reported
not reported
not reported

Reference

Resh and Runeckles (1973)
Heagle and Strickland (1972)
Cojenum et al. (1987)
Hibben and Taylor (1975)
Heagle (197Q)
Tiedemann et al. (1991)
Heagle and Key (1973a,b)
Heagle (1975)
Dohmen (19857)
Tiedemann et al. (1990)
Tiedemann et al. (1990),
Tiedemann et al. (1990)
Manning et al. (1971)


-------
                       TABLE 5-6 (cont'd). OZONE-PLANT-PATHOGEN INTERACTIONS
0\
Host Plant
FACULTATIVE
Corn
Cottonwood
Geranium
Onion
Potato


Soybean
Wheat






Jeffrey pine
Pathogen
FUNGI (cont'd)
Helminthosporium
maydis
Marssonina brunnea
Botrytis cinerea
Botrytis (3 spp. )
Botrytis cinerea
Altemaria solani
Alternaria solani
Fusarium oxysporum
Gerlachia nivalis
Helminthosporium
sativum
Helminthosporium
sativum
Septoria (2 spp.)
Septoria (2 spp.)
Heterobasidium annosum
Effect of Oj on Disease

increased development
increased infection
decreased infection
increased infection and
development
increased infection and
development
increased infection
increased infection
increased infection
increased infection
no effect

increased infection

increased infection
oncreased infection
increased development
Effect of Disease on O3 Response

not reported
not reported
not reported
not reported
not reported
not reported
not reported
increased leaf injury
not reported
not reported

not reported

not reported
not reported
not reported
Reference

Heagle (1977)
Coleman et al. (1988)
Krause and Weidensaul (1978)
Wukasch and Hofstra (1977a,b)
Manning et al. (1969)
Holley et al. (1985)
Bisessar (1982)
Damicone et al. (1987)
Tiedemann et al. (1990)
Tiedemann et al. (1990)

Tiedemann et al. (1991)

Tiedemann et al. (1990)
Tiedemann et al. (1991)
James et al. (1980)

-------
TABLE 5-6 (cont'd). OZONE-PLANT-PATHOGEN INTERACTIONS
3
if
_
OJ










OS
Os


d
£
H
d
O
g
3
o
d
o
#
o
Host Plant
FACULTATIVL FUNGI
Ponderosa pine
White pine



BACTERIA
Alfalfa
Soybean

White bean
Wild strawberry
NEMATQDES
Begonia

Soybean






Tobacco

aBased on studies using the




Pathogen
(cont'd)
Heterobasidiwn annosum
Vertcidadiella procera

Lophodermium pinastre


Xanthomonas alfalfae
Pseudomonas glycinea
Pseudomonas sp.
Xanthomonas phaseoli
Xanthomonas fragariae

Aphelenchoides
fragariae
Belonolaimus
longicaudatus
Heterodera glycines

Paratrichodorus minor

Pratylenchus penetrans
Meloidogyne hapla

protectant EDU (see Section




Effect of 03 on Disease

increased development
slightly increased
incidence
slightly increased
incidence

reduced development
reduced incidence
reduced infection
no effect
reduced incidence

reduced nematode
reproduction
stimulation or no effect

reduced nematode
reproduction
reduced nematode
reproduction
no effect
possible stimulation4

5.3.2.4.1.3).




Effect of Disease on 03 Response

not reported
not reported

not reported


reduced leaf injury
no effect
reduced leaf injury
reduced leaf injury
no effect

reduced leaf injury

not reported

not reported

reduced leaf injury

not reported
increased leaf injury






Reference

James et al. (1980)
Costonis and Sinclair (1972)

Costonis and Sinclair (1972)


Howell and Graham (1977)
Laurence and Wood (1978a)
Pell et al. (1977)
Temple and Bisessar (1979)
Lawrence and Wood (1978b)

Weber et al. (1979)

Weber et al. (1979)

Weber et al. (1979)

Weber et al. (1979)

Weber et al. (1979)
Bisessar and Palmer (1984)







-------
 1     whereas increases were observed in all but four of the studies of facultative fungal pathogens.
 2     Similarly, in four of the five bacterial systems, O3 reduced infection or disease development.
 3     It should be noted that in three of the four studies of obligate fungi on which exposure to
 4     O3 either had no effect or which resulted in stimulated fungal growth the pathogen was a
 5     powdery mildews (Erysiphe, Microsphaerd).  As discussed by Tiedemann et al. (1991), these
 6     species constitute a  special case because they are ectoparasites whose hyphae merely
 7     penetrate the surface epidermal cells of the host plants leaves rather than the mesophyll
 8     tissues within the leaves.  They noted that Heagle and Strickland (1972) observed greater
 9     pustule development of Erysiphe on exposed barley once infection was established, although
10     the pathogen was sensitive during the early  stages of infection.  Tiedemann et al. (1991)
11     suggest that the observed stimulations result from a differential weakening  of the host's
12     resistance response  to the pathogen.
13          In a few of the studies summarized in Table 5-6, effects of disease development on the
14     sensitivity of the host plant to O3 were noted.  Heagle and Key  (1973b) and Resh and
15     Runeckles (1973) confirmed the earlier observation of Yarwood and Middleton (1954)  that
16     infection with obligate rust fungi could reduce the severity of acute injury caused by
17     exposure to O3.  However, with Uromyces on bean, the "protection" was only noted on
18     severely infected leaves (Resh and Runeckles,  1973), and Heagle (1970) observed no such
19     effect with crown rust, Puccinia coronata, on oats.
20          Infection with bacterial pathogens and nematodes also tends to reduce the impact of
21     O3, and almost all studies of the interactions of O3 with virus infections appear to do so.
22     The previous criteria document (U.S. Environmental Protection Agency, 1986) reviewed the
23     supporting evidence from numerous studies with a range of host plants and viruses, and
24     noted only two studies in  which O3 injury was apparently increased by virus infection
25     (Ormrod and Kemp, 1979; Reinert and Gooding, 1978).  However, with tomato infected by
26     mosaic vinises, injury was reduced in the leaves of plants in which viral infection was well
27     established (Ormrod and Kemp,  1979). Two more recent studies have indicated either no
28     effect or variety-dependent increased sensitivity to relatively  high O3 levels.  Heagle et al.
29     (1991, 1992) found no effects of infection with several viruses on the response of two  clonal
30     strains of white clover.  On the other hand, Reinert et al. (1988) reported that three cultivars
31     of burley tobacco responded differently to O3 when infected  with either tobacco etch virus

       December 1993                            5.57      DRAFT-DO NOT QUOTE OR CITE

-------
 1      (TEV) or tobacco vein mottling virus (TVMR).  Although TEV-infection resulted in the
 2      protected all cultivars from O3-induced growth suppression, TVMV infection enhanced the
 3      suppression of the growth of two cultivars, Burley 21 and Greenville 131, but had no effect
 4      on the third, Burley 49.
 5           With the exception of one field study demonstrating the suppression of O3 injury on
 6      tobacco infected with tobacco mosaic virus (Bisessar and Temple, 1977), the other
 7      investigations of virus interactions have all been conducted in laboratory or greenhouse
 8      chambers, which raises the question of their relevance to  field conditions. As noted in the
 9      previous criteria document (U.S. Environmental Protection Agency, 1986), with few
10      exceptions, the reports of viral protection are probably of little commercial significance,  but
11      may provide information at the mechanistic level of plant response.  The same caveat is
12     equally applicable to the significance of protective effects of other obligate pathogens.
13           No studies appear to have been conducted of interactions involving disease-causing
14     mycoplasmas.
15           As in the case of plant-insect interactions, much more systematic study is needed before
16     it will be possible to provide any quantitative estimates of the magnitude of the interactive
17     effects. The patterns of pollutant modification of plant-pathogen relations suggested by
18     Dowding (1988) are partly supported by the limited evidence available for O3, but studies of
19     a wider range of plant-pathogen systems will be needed before it will be possible to provide
20     quantitative generalizations.
21
22      5.4.3.3  Oxidant-Plant-Symbiont Interactions
23           Exposure to O3 can modify the symbiotic relationships between plants and
 24      microorganisms. In the case of Rhizobium, the important nitrogen-fixing symbiont of many
 25      leguminous species, the adverse effects of exposure of the host plant reviewed in the
 26      previous criteria document (U.S. Environmental Protection Agency, 1986) were all observed
 27      at O3 levels of 0.3 ppm or greater.  However, Flagler et al. (1987) observed a consistent
 28      decline in total nitrogen-fixing activity of nodulated soybean roots with increasing
 29     O3 concentrations up to 0.107 ppm (7-h/day seasonal average),  with no effect on specific
 30     nodule activity.  In a greenhouse study of soybean plants exposed at three different growth
 31      stages to a 12 h treatment in which the peak O3 concentration (at 6 h)  was 0.2 ppm, Smith

        December 1993                           5-68       DRAFT-DO NOT QUOTE OR CITE

-------
 1     et al. (1990) observed a 40% decrease in specific nodule activity.  Hence, there is limited
 2     evidence to indicate adverse effects on Rhizobial nitrogen-fixation at O3 levels experienced in
 3     polluted air.
 4          The effects of O3 on mycorrhizal fungal symbioses have been reviewed by Manning
 5     and Keane (1988) and McCool (1988). Seasonal exposures averaging 0.079 ppm O3 resulted
 6     in a  40%  reduction in the growth of the vesicular-arbuscular endomycorrhizal fungus,
 7     Glomus fasciculatus, on soybean roots.  However, mycorrhizal infection lowered the
 8     O3-induced reduction in pod yield from 48 to 25% (Brewer and Heagle, 1983).
 9     Once-weekly exposures of tomato plants to 0.3 ppm for 3 h retarded the early development
10     of the  same fungus on tomato seedling roots, leading to reduced seedling growth (McCool
11     et al.,  1982).  Greitner and Winner (1989) reported that the increased availability of nitrogen
12     to alder seedlings resulting from the presence of root nodules containing the nitrogen-fixing
13     actinomycete, Frankia, enabled plants to recover their photosynthetic integrity rapidly after
14     exposure to O3 However, they did not investigate effects on symbiont.
15          In spite of the inconsistencies in the available evidence, it appears that rhizobial and
16     mycorrhizal growth is likely to be impaired as a consequence of long-term exposure to
17     oxidant stress, probably because of reduced allocation of photosynthate to the root system
18     (Chapter 7, U.S. Environmental Protection Agency, 1986). However, the implications of
19     such effects on mycorrhizae are particularly difficult to predict because of our inadequate
20     understanding of the functioning of the tree root-mycorrhiza-soil system.
21
22     5.4.3.4   Oxidant-Plant-Plant Interactions—Competition
23          In the field, the growth of any plant  is to some extent dependent upon its ability to
24     compete for resources with its neighbors.  Some are better competitors than others for light,
25     water, nutrients, and space.  Grime (1977) characterized as "competitors" those with a rapid
26     growth rate associated with a capacity to adjust to rapidly changing conditions.  Factors such
27     as light or soil nutrients are  not available ad libitum, because of the mutual shading of leaves
28     within the canopy and root competition.  Competition may be either intra- or inter-specific,
29     (i.e., the interference may be caused by  neighboring members of the same species or by
30     neighboring individual of other species).  The planting densities and row spacings adopted
31     for agricultural crops represent compromises between maximizing the number of plants per

       December 1993                           5.59       DRAFT-DO NOT QUOTE OR CITE

-------
 1     unit area and the adverse effects of intra-specific competition. The planting densities and
 2     row spacings adopted for agricultural crops represent compromises between maximizing the
 3     number of plants per unit area and the adverse effects of intra-specific competition. Weeds
 4     are typical interspecific competitors.  Interspecific competition also occurs in mixed plantings
 5     such as grass-clover forage and pasture plantings, and is an important feature of natural
 6     ecosystems.
 7          Although competition from weeds may contribute  more to crop losses on a global scale
 8     than any other factor, no studies appear to have been conducted on the effects of oxidant
 9     pollution on such competition.  On the other hand, a few crop mixtures have been studied.
10     A consistent finding with grass-clover mixtures has been a significant shift in the mixture
11     biomass in favor of the grass species (Runeckles and Bennett, 1977; Blum et al., 1983;
12     Kohut et al., 1988; Rebbeck et al., 1988; Heagle et al., 1989).
13          As the number of competing species increases, the interactions are more appropriately
14     dealt with at the ecological level, but, as  demonstrated by the work of Evans and Ashmore
15     (1992), it is important to recognize that, because of the differential stresses imposed by
16     competition, the impact of O3 on the components of a mixture may not be predictable  on the
17     basis of knowledge of the responses of the individual species grown in isolation. A similar
18     caution must be stated about extrapolating to field conditions results obtained in laboratory
19     studies in which competition may be minimal. However, the development and use of  field
20     exposure systems have permitted many recent  studies of crop species to be conducted at
21     normal planting densities and hence have incorporated interspecific competition as an
22     environmental factor.  On  the other hand, most forest tree studies have tended to be
23      "artificial" in their use of individual seedlings or saplings or spaced trees, even when
24     exposed in open-air  systems (McLeod et al., 1992).
25           The significance of the effects of competitive interactions on the O3 response of the
26     competing species is thus largely unknown except for a few cases involving grass-legume
27     mixtures.  However, these are far from typical because they only involve two  species, one of
28      which is  a legume with unique nitrogen nutrition conferred by the nitrogen-fixing capabilities
29      of Rhizobial symbionts. Hence, at the present time, our lack of knowledge of the effects of
30      O3 on competitive interactions leads to considerable uncertainty in attempting to assess the
        December 1993                          5-70       DRAFT-DO NOT QUOTE OR CITE

-------
 1      impact of O3 on both managed and natural ecosystems, by extrapolation from effects on
 2      individual species.
 3
 4      5.4.4   Physical Factors
 5           The physical components of the plant's aerial environment are light, temperature,
 6      humidity and surface wetness, while the physical, edaphic components affecting the plant
 7      roots are temperature, soil moisture and soil salinity.  The previous criteria document (U.S.
 8      Environmental Protection Agency, 1986) also included soil fertility under this heading; in the
 9      present review, this  topic is dealt with separately in the section dealing with chemical factors
10      (Section 5.4.5).  The effects of the physical climatic factors (light, temperature, and the
11      availability of water) on plant growth and survival are major determinants of the geographic
12      distribution of the earth's natural vegetation and of the distribution of agricultural lands and
13     the suitability of the crops grown on them.  Because of the control that these factors exert
14     over plant growth, their variation, especially in the short term, can be expected to influence
15     the magnitude of plant responses to oxidants.  As in the previous criteria document, the
16     factors are discussed individually, although  their actions on plant growth and sensitivity are
17     closely inter-related. A brief integration of their effects is presented in  Section 5.4.8, which
18     discusses the effects of global climate change.
19           At the tune of the previous criteria document, much of our knowledge of the effects of
20     these factors came from laboratory and greenhouse experimentation which focused the foliar
21     injury response  to high exposures to O3 that exceeded those likely to be encountered in
22     ambient air.  Since then, more information  has become available on growth effects,
23     especially with regard to the key area of the interactions involving drought stress.
24
25     5.4.4.1  Light
26           Light influences plant growth through its intensity, quality (i.e., the distribution of
27     wavelengths), and duration  (i.e., day length  or photoperiod).  Much of the early work on
28     light-oxidant interactions is  largely of academic interest since light intensity and daylength
29     are  uncontrolled in natural field situations.  However, reduced intensities are needed for the
30     production of shade-grown  cigar wrapper tobacco and in many commercial greenhouse
31     floriculture operations, in which photoperiod may also be controlled in  order to induce

       December 1993                           5-71       DRAFT-DO NOT QUOTE OR CITE

-------
 1     flowering.  The general conclusion reported previously (U.S. Environmental Protection
 2     Agency, 1986) is that susceptibility to foliar injury is increased by low intensities and short
 3     photoperiods,  although unpredictable responses had been observed when plants were
 4     subjected to increased or decreased intensities during and after exposure to O3.  One  aspect
 5     of increased susceptibility to low light intensities that needs to be emphasized concerns the
 6     fact that many studies of oxidant effects have been conducted in controlled-environment
 7     chambers in which the light intensities used have rarely  approached those of natural sunlight,
 8     and hence may have magnified the observed responses.  Significant differences in the
 9     amounts of foliar injury were observed on  soybean plants grown in a growth chamber, a
10     shaded greenhouse or in an open-top chamber in the field when subsequently treated  with a
11     standard O3 exposure,  although the growing conditions other than light intensity and  quality
12     were comparable (Lewis and Brennan,  1977).  Factors other than light intensity must have
13     contributed to the observed differences since the descending order of sensitivity was
14     greenhouse-growth chamber-field chamber, although the average light intensities in the
15     greenhouse and growth chamber were 81 % and 18%, respectively, of those  in the field
16     chamber.
17          Reduced light intensities have been measured in open-top chambers in the field,
18     resulting form the build-up of dust on the walls. However,  Heagle and Letchworth (1982)
19     could detect no significant effects on soybean growth and yield in a comparison of plants
20     grown in unshaded open-top chambers  and chambers to which shading cloth was applied.
21          At the mechanistic level,  Darrall  (1989) has reviewed the effects of light intensity and
22     suggests that,  at high intensities, the potential for endogenous oxyradical production is
23     greatest and that  this, combined with the production of oxyradicals from 03, might exceed
24     the leaf's detoxification ability.  However, at lower intensities, decreased carbon assimilation
25     would limit the availability of energy for use in cellular repair.
26          In most  species,  light indirectly plays a major role in the opening and closing of
27     stomata.  Since stomata therefore tend to close at night  and open during the day, light
28     duration to some extent dictates whether or not O3 can be taken  up by foliage from the
29     ambient air.
30
31

        December 1993                           5-72       DRAFT-DO NOT QUOTE  OR CITE

-------
 1     5.4.4.2  Temperature
 2          Temperature affects almost all physical processes and chemical reactions within the
 3     plant.  Hence it is the temperature within the plant tissues that is important.  Although air
 4     temperature dictates the overall heat balance in the surrounding air, the temperature of the
 5     leaf is also determined by the absorption of infra-red radiation during the photoperiod (which
 6     increases the leaf temperature), and the loss  of water vapor through transpiration (which
 7     provides evaporative cooling).  Hence the effects of air temperature per se must be viewed in
 8     the context of these other physical factors.  It is therefore not surprising that the few early
 9     studies of the effects of air temperature alone, using controlled environment chambers, led to
10     variable and conflicting results, as noted in the previous criteria document (U.S.
11     Environmental Protection Agency, 1986).  In most of these studies, the relative humidity
12     (RH) and light intensity were held constant.  In water-saturated air with a relative humidity
13     of 100%, the absolute humidity (or water vapor pressure) increases with temperature. Such
14     increases occur at all RHs.  Therefore, at constant RH, the increase in absolute humidity
15     (or vapor pressure) with temperature, in turn, increases the vapor pressure deficit (VPD)
16     (i.e., the difference between the absolute humidity) (or vapor pressure) and that of
17     completely saturated air at the same temperature.  Since VPD controls the rate of evaporation
18     of water, at constant RH the effects of temperature are unavoidably confounded with effects
19     on VPD.  In a recent study with tomato seedlings, in which differences in VPD at different
20     temperatures were  minimized, Todd et al. (1991)  showed that,  out of 11 growth variables
21     measured, the only significant modifications of the effects of O3 caused by temperature were
22     on stem fresh weight and specific leaf area (leaf area/leaf dry weight).  The authors suggest
23     that  VPD probably plays a more important role in determining sensitivity to O3 than
24     temperature.
25          Although transpiration rate is dependent on VPD, it is also regulated by the  opening
26     and closing of stomata on the leaf surface, and factors such as O3  that cause stomatal closure
27     will  indirectly cause leaf temperature to rise. Such stomatal  and temperature changes have
28     been observed during exposure to  O3  (Matsushima et al.,  1985; Temple and Benoit, 1988).
29          An important O3-temperature interaction affecting trees and other woody perennials is
30     winter hardiness.  Several studies have shown that exposures to O3 at realistic levels may
31     reduce the cold- or frost-hardiness of plants, as reviewed by  Davison et al. (1988).  Using

       December 1993                           5.73       DRAFT-DO NOT QUOTE OR CITE

-------
 1     the pea plant as a laboratory model, Barnes et al. (1988) showed that daily 7-h exposures to
 2     0.075 or 0.09 ppm O3 for seven days significantly reduced plant survival after exposure to
 3     night-time temperatures that fell from 2 °C to -4 °C over a 2-h period and were than held at
 4     -4 °C for a further 4 h.
 5          Various responses of coniferous trees to the exposure to O3 during the growing season
 6     and freezing temperatures during the following winter have been reported. With Norway
 7     spruce, Eamus and Murray (1991)  found that the recovery  of photosynthetic rates after
 8     freezing was slower in O3-treated seedlings.  Brown et al.  (1987) and Barnes  and Davison
 9     (1988) observed  severe necrosis of the older  needle classes of seedlings of some Norway
10     spruce clonal saplings exposed to O3 and then to freezing temperatures although other clones
11     showed no effect.  Increased winter injury on plants exposed to O3 was also observed with
12     Sitka spruce (Lucas et al., 1988) and red spruce (Fincher et al., 1989).  With loblolly pine,
13     Edwards et al. (1990) observed variable results, but Chappelka et al. (1990) reported that a
14     late winter frost  resulted  in severe tip die-back of the youngest needles of seedling trees
15     exposed to 1.7 (350 ppm-h) and 2.5 (433 ppnvh) times the ambient (272 ppm-h)
16     O3 concentration during the previous growing season, in contrast to the effects observed on
17     Norway spruce.  The response also varied with plant genotype.  A reason for the difference
18     may be that, in the study with Norway spruce, the  freezing period occurred soon after
19     exposure to elevated O3 levels, while in the loblolly pine study the frost occurred in late
20     winter.  The diversity of results led Eamus and Murray (1991) to develop a conceptual
21     framework which recognizes that even  in severe  winters there are brief periods of mild
22     temperatures that induce  partial dehardening.  While O3 decreases frost hardiness per se,
23     it also increases  the trees' predisposition to dehardening given favorable conditions during
24     winter.  Such dehardening puts O3-exposed trees at greater risk from subsequent low
25     temperatures.
26           In a greenhouse study with one-year old red spruce seedlings, Neighbor et  al.  (1990)
27     reported briefly  that decreasing the level of nitric oxide at the time of exposure to
28     O3 prevented the appearance of O3-induced frost injury. They suggest that the effects
29     attributed to O3  are probably due to the combination of O3 with traces of NO above a critical
30     level. However, this effect has not apparently been investigated further.
        December 1993                           5.74      DRAFT-DO NOT QUOTE OR CITE

-------
 1           In a study of the sub-tropical trees, citrus and avocado, in Florida, Eissenstat et al.
 2      (1991) found that, although O3 could reduce frost hardiness, the effects were subtle, and the
 3      authors concluded that the likelihood that frost resistance is adversely affected by current
 4      O3 levels is slight.
 5           The general consequences of global warming on O3 responses are discussed in
 6      Section 5.4.8.
 7
 8      5.4.4.3  Humidity and Surface Wetness
 9           A review of early investigations led to the conclusion that, in general, high relative
10      humidity (RH) tends to sensitize plants to O3 (U.S. Environmental Protection Agency, 1986).
11      Such a conclusion is supported on mechanistic grounds.  Mclaughlin and Taylor (1982)
12      studies indicated that measured O3 uptake by bush bean plants increased with RH, and there
13      are several reports that, at high RH, the rapid decrease in stomatal conductance caused by
14     O3 at lower relative humidities is inhibited (Otto and Daines, 1969; Rich and Turner, 1972;
15     Elkiey and Ormrod, 1979).  However, stomatal responses to O3 show considerable variability
16     among species and even among cultivars of the same species (Elkiey and Ormrod, 1979), and
17     hence  it is to be expected that the patterns  of the O3-RH interaction may not always be as
18     clear.  Thus with yellow poplar,  five consecutive daily exposures to 0.15 ppm for 7 h at
19     either  40% or 80% RH revealed  considerable variation in stomatal conductance (Jensen and
20     Roberts, 1986).  At 40% RH, there was a tendency for O3 to  cause a decrease hi
21     conductance during the later exposures.  Nevertheless, at 80% RH the conductances were
22     generally greater and tended to increase during the later exposures.
23          Surface wetness also influences the foliar uptake  of O3 although there appear to have
24     been no studies undertaken to investigate the consequences of such uptake.  Until recently, it
25     has been suggested that O3 uptake is reduced when foliage is wet because the stomata may be
26     covered with water (Hicks et al., 1987). However, Fuentes and Gillespie (1992) reported
27     that both wetness from dew or raindrops on the upper surface of maple leaves can
28     significantly increase O3 uptake.  While this may partly be due to a stomatal response to
29     resulting increases in RH, the fact that increased uptake occurred in darkness when the
30     stomata were largely closed led them to suggest that direct uptake into the surface water is
        December 1993                           5.75       DRAFT-DO NOT QUOTE OR CITE

-------
 1     the more important mechanism. However, no information is yet available as to the
 2     consequences of such deposition.
 3
 4     5.4.4.4  Drought and Salinity
 5          Short- and long-term variations in the availability of soil water have a profound
 6     influence on plant growth.  In some agricultural situations, the use of irrigation may
 7     eliminate drought stress.  However, the growth of crops and natural vegetation in many areas
 8     will adversely affected by the varying degrees of water shortage that occur,  both during a
 9     growing season and from year to year. The previous criteria document (U.S. Environmental
10     Protection Agency,  1986) summarized earlier studies and concluded that drought stress
11     reduced the magnitude of adverse effects  of 03 including injury and growth  or yield
12     reductions.  The effect was attributed  to an increased rate of stomatal closure in
13     drought-stressed plants in response to  O3  that effectively reduced uptake of the pollutant.
14     These conclusions were based almost  exclusively on studies with crop species.  Since then, a
15     number of studies with tree seedlings  and further studies with crops species have shown that
16     the interaction between drought and O3 is more complex  and variable than originally thought.
17           Heagle et al. (1988a) summarized the results of investigations  into the drought-
18     O3 interaction in six soybean and three cotton studies, and one study each of alfalfa and a
19     clover-fescue mixture. These studies  were undertaken as part  of the National Crop Loss
20     Assessment Program  (NCLAN) (Heck et al., 1984).  The results of these investigations are
21     included in Table 5-7. Significant interactions between O3 and drought stress (soil moisture
22     deficit, SMD) were reported only in three soybean and two cotton studies and the alfalfa
23      study.  The interaction was usually revealed by the fact that the clear negative relationships
24      between yield and O3 exposure observed with watered plants was either much reduced or
25      could not be demonstrated with drought-stressed plants, bearing in mind that in most of these
26      situations the yields were already depressed by the SMD. As a result, the lack of any
27      significant response to O3 in some cases  with such stressed plants reflects the decreased
 28      range of yield responses within which an O3 effect could operate.  However, as shown in
 29      Table 5-7, Heggestad et al. (1988) found with Forrest  soybean that SMD significantly
 30     enhanced the effects  of low O3 exposures. Heagle et al. (I988a) therefore  were forced to
 31      conclude that the suppression of the response to O3 caused by drought appeared to be

        December 1993                           5-76       DRAFT-DO  NOT QUOTE OR CITE

-------
TABLE 5-7.  FIELD STUDIES OF OZONE-DROUGHT STRESS INTERACTIONS IN CROP SPECDZS
I
I— »







1
^


d
g
H
1
d
o

1
0
Estimated Yield Loss (%) per Seasonal Mean
O3 Concentration (ppm)
Crop/Cultivar Year
Soybean
Williams 1982

Williams and 1983
Corsoy 79
Williams

Forrest 1982

Davis 1983


Yield
Davis 1984

Corsoy 79 1986

Young 1986

Response

Yield

Yield
Yield
Root length
Root length
Yield
Yield
Yield
DS

DS
Yield

Yield
Yield
Yield

Significant
Interaction

No

WW
DS
WW
DS
WW
DS
WW



No

WW
DS
No

0.04

7

7
6

0.05

13

13
11
no
0.06

19

18
15
significant O3
[33 36
3
13
4



4

2
0
6

9
21
7


no
7

4
0
11

21
28
12


significant 03
12

8
0
17

0.07

24

24
19
effect
/»
52]3
39
35
16


effect
18

13
0
25

0.08

30

30
23


60
41
21



24

21
1
34

Reference

Heggestad et al. (1985)
Heggestad and Lesser (1990)

Heggestad and Lesser (1990)
Heggestad et al. (1988)

Heggestad et al. (1985)
Heggestad and Lesser (1990)
Heagle et al. 1987)



Heagle et al. (1987)

Irving et al. (1988)

Miller et al. (1989)


-------
S5
8
u
• >.  M
81
O K
^1
0(2
S3 *
O.S
81
      i§
      % g
      3 i
       o
            O
            o
            2

          c/
Cultivar
C
December 1993
                 

                 •a
                 u
                 !
                          £
282
^,  »«H ^/
   ***iS ^"^
•a  -a is
"S  -S «
43  « ja
III
H  DC tS
                 82 R  s
                 3^ ?
  S
                                    •a
                                    u
                                    t
                                    ss

                 en I-H vo  r-
                   c«  o
                                    55 S5
                                           i
                                           1
                      as
                                           CSt-
                                           o o
                 cs
                     000000
                     O\O\O\
                     (S  en 
-------
 1      dependent on the severity of the SMD-induced stress.  This conclusion was supported
 2      empirically by the fact that the interaction was observed in hot, dry summers, but not in
 3      cool, cloudy seasons.  However, because different measures of SMD or SMD-induced stress
 4      were used in different studies, it is not possible to quantify the relationship between the
 5      suppression the O3 response and the level of drought stress.  Furthermore, soil conditions at
 6      different sites and the depth of the water table in the soil also appeared to influence the
 7      interaction through effects on the vertical distribution of root growth (Heggestad et al.,
 8      1988).  Moser et al.  (1988) showed that impact of O3  on the growth and yield of bush bean
 9      plants was reduced more by a period of SMD early  in the reproductive phase of growth than
10     at a later stage.
11           A retrospective analysis of three years' data involving four soybean cultivars led
12     Heggestad and Lesser (1990) to conclude that, regardless of whether or not drought stress
13     reduced the impact of ozone, in the majority of cases the yield curves  showed comparable
14     slopes with increasing O3 exposure.  This led them to  question the justification for the
15     20% reduction in sensitivity to O3 used  by King  (1988) in modelling the
16     drought-O3 interaction.
17          Brennan et al. (1987) suggested that the normal experimental protocols used in most
18     NCLAN studies, which called for the use of irrigation to avoid possible complications due to
19     drought, might have biased the yield loss data for soybean because it increased plant
20     sensitivity to O3.  However, Heggestad  and Lesser (1990) found no evidence to support this
21     suggestion hi view of the comparable estimates of yield losses predicted by the O3-response
22     curves.
23          Bytnerowicz et al. (1988) found no interaction between SMD and O3 in 18 desert
24     annual species. However, moderate SMD rendered the tropical fibre plant, kenaf, less
25     sensitive to O3 although sensitivity was  enhanced by sever water stress (Kasana, 1992).
26     A field survey of milkweed plants in two areas in the  mid-Ohio River Valley revealed much
27     less foliar injury attributable to O3 in 1988, a dry year in which the maximum  concentration
28     recorded nearby reached 0.2 ppm, than in 1989, a year with ample precipitation and  a nearby
29     maximum of only 0.12 ppm (Showman, 1991).
30          Although there have been several recent studies of the effects of O3 exposure and
31     drought stress on tree species, they have little in common with respect to the treatments

       December 1993                           5.79      DRAFT-DO NOT QUOTE OR CITE

-------
 1     applied or the measurements made.  However, clear demonstrations of significant interactions
 2     have been obtained with beech, poplar and loblolly pine seedlings.  Davidson et al.  (1992)
 3     found that although O3 reduced root growth in well-watered plants, SMD reversed this
 4     inhibition and led to slight O3-induced stimulations.  Drought reduced foliar injury caused by
 5     O3 to poplar (Harkov and Brennan,  1980), ponderosa pine (Temple, 1992) and loblolly pine
 6     (Meier et al., 1990).  In poplar, the effect was attributed to the reduced stomatal conductance
 7     observed which reduced O3 uptake.  Similar effects on stomatal conductance were observed
 8     in Norway spruce and sitka spruce (Dobson et al.,  1990).  In ponderosa pine,  SMD also
 9     countered the inhibitory effects of O3 on needle growth and retention (Temple et al., 1993).
10     Tseng et al. (1988), however,  observed no effects of O3 on Fraser fir grown under three
11     levels of SMD.  No consistent patterns were found with various physiological  measurements
12     made on red spruce seedlings subjected to both O3 and drought (Roberts and Cannon, 1992).
13     Lee et al. (1990) observed reduced root conductivity in the second drought cycle following
14     exposure to O3.
15           Thus there is some evidence from tree species to support the view that drought stress
16     may reduce the impact of O3.  However, the work with trees provides no additional
17     information to help in resolving the quantitative nature of the drought-O3 interaction.
18           Although drought stress may be the result of insufficient rainfall, conditions of effective
19     SMD may also be induced by  excessive soil salinity.  Laboratory  studies showed that
20     increased salinity could reduce the impact of O$ on injury and yield on various crops, as
21     reviewed in the previous criteria document (U.S. Environmental Protection Agency, 1996).
22     However, in a more recent field study with alfalfa, Olszyk et al. (1988)  found no overall
23     interaction between O3 and salinity on growth or yield.  Although salinity decreased the
24     number of empty nodes caused by exposure to above  ambient levels of Oj, the effect was
25     only  statistically significant for the second of four harvests. In general,  salinity was found to
26     be a  more harmful to alfalfa growth than exposure to  O3,  but, as  pointed out  by Olszyk et al.
27      (1988), the amount of information available is insufficient to permit the  development of
28      models for estimating losses due to O3-salinity combinations.
29           The bulk of the available evidence supports the view that drought stress  may  reduce the
30      impact of O3 on plants.  However, it must be emphasized that, in terms of growth and
        December 1993                           5-80       DRAFT-DO NOT QUOTE OR CITE

-------
 1     productivity, any "protective" benefit will be offset by the effects of SMD per se, as noted in
 2     the previous criteria document (U.S. Environmental Protection Agency, 1986).
 3          The O3-water interaction is not confined to the effects of SMD on direct plant response
 4     to O3.  Numerous studies have shown that O3 may affect various aspects of plant water
 5     status,  including water use efficiency (WUE), the ratio of the rates of photosynthetic carbon
 6     gain and transpirational water loss.  For example, Reich et al. (1985) observed that daily
 7     exposures to 0.13 ppm O3 for 6.8 h resulted in  a 25 % reduction in WUE in well-watered
 8     Hodgson soybean, when  compared to exposure to 0.01 ppm.  Similar findings have been
 9     reported for alfalfa (Temple and Benoit, 1988) and radish (Barnes and Pftrrmann,  1992).
10     However, WUE is a complex resultant of both stomatal conductance and the activity of the
11     photosynthetic system, both of which may be independently affected by O3. Genetic or
12     environmentally induced  difference  in the relative sensitivities of the stomatal and
13     photosynthetic components  will dictate the nature and magnitude of any effect of O3 on
14     WUE.  Thus,  with radish and soybean, Greitner and Winner (1988) observed effects on
15     stomatal conductance and photosynthetic CO2 assimilation that translated into O^-induced
16     increases in WUE, they point out, that this advantageous increase far outweighed the adverse
17     effects of O3 on growth.
18          However, these reports concern herbaceous weedy species, and there appears to be only
19     one  report concerning tree  species.  Johnson and Taylor (1989)  reported that exposure to
20     higher than ambient levels of O3 results in adaptation to a more efficient use of water by the
21     foliage of loblolly pine seedlings. The corollary to this observation is the trees exposed
22     continuously to low O3 levels may be more sensitive to recurrent drought stress than those
23     grown under higher exposure levels.  The corollary to this observation is that trees exposed
24     continuously to low O3 levels may be more sensitive to recurrent drought stress than those
25     grown under higher exposure levels.  As with most studies of tree species, these observations
26     were made on tree seedlings, and their relevance to mature trees has still to be established.
27          It is therefore clear that not only does drought have a pronounced effect on the response
28     of most species to O3, but that O3 also may also modify plant water relations including
29     conferring drought tolerance.  However, more study will be needed before it will be possible
30     to generalize about the implications of the latter effect, and its importance to forest
31     ecosystems.

       December 1993                           5-81       DRAFT-DO NOT QUOTE OR CITE

-------
 1     5.4.5   Nutritional Factors
 2          All land plants require an adequate supply of essential mineral elements from the soil in
 3     order to avoid adverse effects on growth and survival resulting from mineral deficiencies.
 4     Two of the essential elements needed for growth are nitrogen and sulfur, and although these
 5     are normally obtained from the soil through the root system, the plant's needs can, at least in
 6     part, also be met by the uptake of pollutant gases such as NO2 and SO2.  Other nutrients
 7     such as phosphorus, potassium, magnesium and calcium are generally only available from the
 8     soil.
 9          A supply of elements such as nitrogen, potassium,  phosphorus, sulfur, magnesium  and
10     calcium is essential for plant growth, but optimal growth requires that the supply be
11     balanced; with insufficiency (or excess) of any of them,  growth will be sub-optimal.  Not
12     surprisingly, therefore, nutrient imbalance has been shown to affect response to O3, although
13     the previous criteria document (U.S. Environmental Protection Agency, 1986) concluded that
14     work to that date had not clarified the relationship between soil fertility and sensitivity to O3,
15     largely because of the differences in nutrients and species selected for study and the
16     experimental conditions used.   This conclusion is still valid,  in spite of the results of a
17     limited number of more recent studies, and is not surprising in view of the vast number of
18     possible permutations and combinations of nutrient elements and their levels that may exert
19     effects on O3 response.  A comprehensive summary of the relevant studies is presented in
20     Table 5-8.
21           Most information concerns nitrogen.  Inspection of Table 5-8  shows that in three of the
22      13 studies,  increased  N supply increased susceptibility to foliar injury or enhanced adverse
23     effects of O3 on growth; three of the studies showed the opposite effects; in three studies,
24     injury was greatest at normal N levels and less at lower or higher levels; in one study, injury
25     was least at normal N levels; and in three studies, no interactions were observed.
26     Knowledge of the tissue N levels resulting from the fertilizer treatments,  as recommended by
27     Harkov and Brennan  (1980), might resolve these contradictions, but these were not reported
28      in most studies.  The  contradictory evidence for tobacco was attributed by Menser and
29      Hodges (1967) do the different cultivars used.
        December 1993                           5-82      DRAFT-DO NOT QUOTE OR CITE

-------
               TABLE 5-8.  OZONE-SOIL NUTRIENT INTERACTIONS
                       Based in part on Cowling and Koziol (1992)
 Species
     Response to Increase in
         Nutrient Level
                  Reference
 Nitrogen (N)
  Loblolly pine

  Ponderosa pine
  Poplar

  Yellow poplar
  Ladino clover/tall fescue
    Mangel
    Radish
    Spinach
    Tobacco
Decreased reduction of growth
due to O3
No injury or growth interactions
Maximum injury in mid range but
no growth interaction
No growth interaction
No growth interaction
Increased injury
Increased reduction of growth due
toO3
Reversal of reduction of shoot
growth due to O3
Increased injury
Decreased injury
Minimum injury in mid range
Maximum injury in mid range
Maximum injury in mid range
       Tjoelker and Luxmoore (1991)

       Bytnerowicz et al. (1990)
       Harkov and Brennan (1980)

       Tjoelker and Luxmoore (1991)
       Monies et al. (1982)
       Brewer et al. (1961)
       Ormrod et al. (1973)

       Pell et al. (1990)

       Brewer et al. (1961)
       Menser and Street (1962)
       Macdowall (1965)
       Leone et al.  (1966)
       Menser and Hodges (1967)
 Phosphorus (P)
  Radish
  Tomato
No growth interaction
Increased injury
        Ormrod et al. (1973)
        Leone and Brennan (1970)
 Potassium (K)
   Norway spruce

   Pinto bean
   Soybean
Decreased reduction of CO2
assimilation due to O3
Decreased injury
Decreased injury
        Keller and Matyssek (1990)

        Dunning et al. (1974)
        Dunning et al. (1974)
 Sulfur (S)
  Bush bean
Decreased injury
        Adedipe et al. (1972)
 Magnesium (Mg)
   Loblolly pine
No growth interaction
        Edwards et al. (1992b)
 General fertility (N-P-K)
   Bush bean
   Soybean
Decreased injury
Maximum injury and growth
reduction in mid range
        Heck et al. (1965)
        Heagle (1979)
December 1993
             5-83
DRAFT-DO NOT QUOTE OR CITE

-------
 1          The limited evidence for phosphorus, potassium and sulfur consistently indicated a
 2     decrease in sensitivity with increased nutrient level.  With respect to general fertility, both
 3     studies listed in Table 5-8 revealed decreased sensitivity to O3 at high levels of nutrient
 4     supply, although with soybean, nutrient-deficient plants also showed decreased sensitivity.
 5     Heagle (1979) found that although injury and growth reductions tended to be greatest at
 6     nonnal levels of fertility, the effects were dependent upon the rooting medium used; in media
 7     containing peat,  the impact of O3 on growth was least at the lowest fertility level.
 8          Cowling and Koziol (1982) have suggested that, in spite of the apparent contradictory
 9     evidence regarding the effects of nutrition on O3 response, there is evidence to support the
10     hypothesis that differences in sensitivity are ultimately linked to changes in the status of
11     soluble carbohydrates in the plant tissues (Dugger et al., 1962).  However, this hypothesis
12     has yet to be systematically tested.
13          Nutritional nitrogen and sulfur can also be supplied directly to foliage in the form of
14     nitrogen and sulfur oxides.  The interactions of these gaseous pollutants with O3, dealt with
15     in the  next section, focus on toxic rather than nutritional effects.  However, one example of a
16     beneficial effect concerns nitrogen pentoxide, N2O5. Since N2O5 is produced in trace
17     amounts by high voltage corona discharge O3 generators, it may contaminate O3 produced
18     from air by such generators for use in studies of effects of O3 on vegetation, unless the
19     O3 stream is first passed through a water scrubber.  Brown and Roberts (1988) reported that
20     deposition of the nitrate formed by hydration of trace amounts of N2O5 in unscrubbed
21     O3 significantly increased the nitrogen status of the exposed plants, which may have
22     confounded the effects attributed to O3.
23
24      5.4.6    Interactions with Other Pollutants
25           The concurrent or sequential exposure of vegetation to different gaseous air pollutants
26      has been found to modify the magnitude and nature of the response to individual pollutants.
27      Some of the early work on the effects of gaseous pollutant combinations, reviewed in the
28      previous criteria document (U.S. Environmental Protection Agency, 1986), is of academic
 29     interest with little relevance to the present review  because of the levels of exposure and the
 30     exposure profiles used  and the fact that the experimental regimes usually involved concurrent
 31      exposures to two or more pollutants repeated daily. Lefohn and Tingey (1984) and Lefohn

        December 1993                           5-84        DRAFT-DO NOT QUOTE OR CITE

-------
 1      et al. (1987) reviewed the patterns of co-occurrence of O3, SO2, and NO2 in urban, rural,
 2      and remote sites in the United States for the years 1978 to 1982 and found that
 3      co-occurrences were usually of short duration and occurred infrequently.  They noted that the
 4      most frequent types of co-occurrence were either purely sequential or a combination of
 5      sequential and overlapping exposures of short duration. Accordingly, the present review will
 6      focus on the evidence  from experiments which simulated these naturally occurring patterns of
 7      combined exposure or at least which used exposure levels in the ranges of those occurring  in
 8      polluted air. An exception is the co-occurrence of O3 and PAN, which are both components
 9      of photochemical oxidant.
10           Over the past decade, the effects of pollutant mixtures have been reviewed by
11      Wolfenden et al. (1992), Shriner et al.  (1990), Mansfield and McCune (1988), Torn et al.
12      (1987), Lefohn  and Ormrod (1984), Reinert (1984), and Runeckles (1984).
13
14      5.4.6.1    Oxidant Mixtures
15           Because of their photochemical origins, elevated levels of O3 and PAN can occur
16     simultaneously. There appear to have been no further investigations of the effects  of
17     simultaneous or sequential exposures since the limited number of studies  reviewed  in the
18     previous criteria document (U.S. Environmental Protection Agency, 1986). Hence, there is
19     no reason to question  the general conclusion, based on the work of Tonneijck (1984) and
20     Nouchi et al. (1984), that the two gases tend to act antagonistically in both concurrent and
21      sequential exposures.  Hydrogen peroxide, H2O2, is also a component of photochemically
22     polluted atmospheres.  Although Ennis et al.  (1990) reported reduced stomatal conductances
23     in red spruce needles  exposed to a mixture of 63, SO2 and H2O2, no studies  have  been made
24     of O3/H2O2 interactions.
25
26     5.4.6.2    Sulfur Dioxide
27          Since SO2 originates from point sources of combustion, the occurrence of high ambient
28     concentrations at a given location is usually episodic because of its dependence upon wind
29     speed, wind direction, and distance from the source.  However, aggregations of point sources
30     can lead to more widespread but less marked increases in ambient SC^ levels.  Thus the
31     potential exists  for elevated O3 exposures to be superimposed on patterns of SO2 ranging

       December 1993                          5-85      DRAFT-DO NOT QUOTE OR CITE

-------
 1      from severe fluctuations to almost steady low-level concentrations.  Concern over the
 2      importance of O3-SO2 interactions dates from the observations of Menser and Heggestad
 3      (1966) that simultaneous exposures of tobacco to SO2 and O3 acted synergistically (i.e., the
 4      effects of the mixture were greater than the sum of the responses to either pollutant alone).
 5      Indeed, in the Menser and Heggestad study, foliar  injury was found to result from exposure
 6      to mixtures although exposures to either gas alone at the same concentrations as in the
 7      mixtures did not result in injury.
 8           Although much of the early work was concerned with foliar injury responses  to
 9      simultaneous exposures to high levels of O3 and SO2,  more recent studies have tended to
10      focus on the consequences of repeated exposures to lower level mixtures or sequences on
11      growth or yield. Several have been aimed at obtaining statistical evidence for the existence
12     of interactions.  For example, Ashmore and Onal (1984), studying  six cultivars of barley,
13     found that SO2  at 0.065 ppm for 6 h, an exposure that induced no adverse effects, acted
14     antagonistically to a 6-h exposure to 0.18 ppm O3, causing significant decreases  in foliar
15     injury, ranging  from 46% to as much as 95%.  However,  only one cultivar, Golden Promise,
16     showed a significant interaction on yield, with SO2 completely reversing the decrease caused
17     by O3 alone. The results could not be explained by effects on stomatal uptake since stomatal
18     conductances were found to be highest in the mixture.  In contrast, with pea, Olszyk and
19     Tibbetts (1981) reported that O3+SO2 caused the same degree of stomatal closure as SO2
20     alone. A similar antagonism to that observed on Golden Promise was also observed in a
21     field study of "Arena" barley (Adaros et al., 1991a) and of spring rape (Adaros et al.,
22      1991b).  However, with "Tempo" spring wheat, a synergistic interaction was  observed:  the
23     adverse effect of O3 on yield (-26%) was increased to -38% by SO2 which by itself only
24     reduced yield by 7%  (Adaros et al.,  1991a). On the other hand, neither Amundson et al.
25      (1987) nor Kohut et al. (1987) observed any interaction in a field study with "Vona" winter
26     wheat.  Irving  et al. (1988)  observed no interaction on field corn.
27           In a series of experiments in which exposure to O3 or an O3/SO2 mixture was preceded
28     by exposures to SO2 alone,  an antagonistic response was observed on foliar injury to white
 29      bean (Hofstra and Beckerson,  1981). In contrast, the responses of cucumber and radish were
 30      synergistic, while there was no interaction on soybean or tomato.  However, when followed
        December 1993                           5-86      DRAFT-DO NOT QUOTE OR CITE

-------
 1     by exposure to an O3/SO2 mixture, S02 pretreatment resulted in an increase in injury to
 2     white bean, decreases on cucumber and tomato, and no effect on soybean and radish.
 3          Field studies with soybean using an air-exclusion system to provide a range of
 4     exposures to O3  and SO2 at ambient and sub-ambient levels revealed an antagonistic
 5     interaction on yield at low concentrations (Jones et al.,  1988).  However, Kress et al. (1986)
 6     found no interaction in a soybean field study using open-top chambers.  No interactions were
 7     found with potato (Pell et al., 1988) or with a red clover-timothy forage mixture (Kohut
 8     etal.,  1988).
 9          From the foregoing, it is apparent that no clearer pattern of the interactive effects of
10     O3 and SO2 on crops has emerged since the previous criteria document (U.S.  Environmental
11     Protection Agency,  1986).  The same is true for the responses of tree species.
12          With tree seedlings, Chappelka et al. (1988a) observed no interaction on white ash.
13     Although a synergistic interaction was found on root growth of yellow poplar (Chappelka
14     et al.,  1985), only additive interactions were found on the growth of other parts of the plant.
15     In a unique study, Kargiolaki et al. (1991) noted that SQ2 reduced the accelerated  leaf
16     senescence caused by O3 on two poplar clones, but had no effect on other clones.  They  also
17     observed additive or less than additive interactions on the formation of intumescences, due to
18     hypertrophy of the stems, and bark cracking. They attributed the differences in clonal
19     response to differences in the levels of pollutant-induced ethylene evolution.
20          Sulfur dioxide reversed the inhibition of photosynthesis caused by exposure to (Jj in
21     two  lichen species, Flavoparmelia caperata and Umbilicaria mammulata (Eversman  and
22     Sigal,  1987).
23          Several studies have attempted to quantify the magnitudes of joint responses to O3 and
24     SO2. The earliest (Macdowall and Cole, 1971) showed that the synergistic injury  response
25     of tobacco occurred  at concentrations of SO2 less than the threshold for SO2 injury,  but not
26     less  than the O3 threshold.  Oshima (1978),  working with kidney bean, found that the
27     synergistic reduction due to intermittent exposures to O3 was linear through a range  of
28     O3 concentrations achieved by varying degrees of filtration of ambient air (expressed as 10 to
29     90 ppm-h of concentrations greater than zero), although the threshold for an O3 response was
30     approximately 47 ppm-h.
       December 1993                           5.37      DRAFT-DO NOT QUOTE OR CITE

-------
 1          A selection of statistical models of injury- or yield responses to O3/SO2 is listed in
 1     Table 5-9.  It is immediately apparent that the models reveal no consistent patterns of
 3     response.  In part, this is because they were developed on the basis of individual experiments
 4     conducted under different environmental conditions at different locations in different years.
 5     Although each model was statistically significant, it was based on a unique data set.  One
 6     study with soybean indicated an antagonistic interaction (Heagle et al., 1983) but another
 7     indicated no interaction (Kress et al., 1986). Cucumber (Hofstra et al., 1985) and snap bean
 8     (Heggestad and Bennett,  1981) were  reported to respond synergistically, while white bean
 9     responded antagonistically (Hofstra et al.,  1985).
10          All that can be concluded from  these studies is that the type of interaction, and whether
11     or not one exists, is probably highly  dependent upon  species and cultivar,  and possibly
12     dependent upon other environmental  variables. The available evidence is insufficient to be
13     able to decide in which way,  and to what extent, SO2 exposure will influence the effects of
14     O3 on a particular species or  cultivar at a particular location.  The original observations of
15     synergism (Menser and Heggestad, 1966) certainly is not a general response.
16
17     5.4.6.3  Nitrogen Dioxide
18           As with SO2, most of the few studies of O3/NO2 interactions that have utilized realistic
19     concentrations have involved  mixtures of the pollutants.  Adaros et al. (1991a) found in a
20     2-year study of two cultivars  each of barley and spring wheat that significant interactions
21     could  only be detected on wheat yield in one growing season.  With both cultivars the
22     interaction was antagonistic.  NO2 also reduced the adverse effect of O3 on  the yield of
23     spring rape (Adaros et al.,  1991b).   Foliar injury to sunflower caused by daily exposures to
24     O3 (0.1 ppm,  8 h) was increased by  continuous exposure to 0.1 ppm NO2 (Shimizu et al.,
25     1984). Plant dry weight was decreased by O3 + NO2 relative to growth in O3 alone, but
26     since O3 exposure resulted in a slight increase in dry weight relative to the controls, the
27     growth in the mixture and  in the controls did not differ significantly.
28           The results of a study of seven tree species exposed to 0.1 ppm  Qj and/or 0.1 ppm
29     NO2 for 6 h/day for 28 days (Kress  and Skelly,  1982) were reported in detail in the previous
30      criteria document (U.S. Environmental Protection Agency, 1986).  However, although
31      several growth interactions were noted in the review, the only statistically significant effect

        December 1993                           5-88      DRAFT-DO NOT QUOTE OR CITE

-------
oo
                            TABLE 5-9.  SOME STATISTICAL MODELS OF COMBINED OZONE AND
                                                    SULFUR DIOXIDE RESPONSES
S"
Co
\o
OJ
Species
Corn
Golden Jubilee
Type of
Interaction
Synergistic
Model
Injury=-11.39+5.4711n(IHT)-9.59[03]+11.81[S02]-86.63[SOJ2+428.95[03][S02]
Reference
Deveau et al.
      Cucumber
      National Pickling
Snap bean
Maple Arrow
interaction
White bean
Seafarer
      Norchip
              (IHT=initial plant height, used as a covariate; [O3] and [SOJ: ppm)


Synergistic     Injury=2.70-f 1.95 n; atfSOJ=0.10 ppm
              Injury=2.40+0.21 n; at[SOJ=0.05 ppm
              Injury=2.39+0.39n; at [SO2]=0.03 ppm
              Injury =1.86+0.166 n; at [SOJ=0.02 ppm
              (n=number of daily 8-h SO2 exposures; O3 exposure:  0.15 ppm, 6 h)


Additive; no    Injury=4.44+34.19[O3]+19.98[SO2]([O3] and [SOJ:  ppm)
Antagonistic   Injury=6.31-0.90 n; at [SO2]=0.10 ppm
             Injury=5.95-0.45n; at [SO2]=0.05 ppm
             (n=number of daily 8-h SO2 exposures; O3 exposure:  0.15 ppm, 6 h)


Additive; no   Yield= 1.27-0.0037[O3]+0.00092[SO2]
interaction     (Yield=number of Grade #1  tubers per plant; [Og]:  ppm, 10 h/day seasonal mean;
             [SOJ:  ppm, 3 h/day)
                                                                                                                (1987)

                                                                                                                Hofstra et al.
                                                                                                                (1985)
Deveau et al.
(1987)a


Hofstra et al.
(1985)
                                                                                                                Pell et al. (1985)
                         Antagonistic   Polynomial model:
                                      Yield=534.5-3988.6[O3]-479.7[SOJ+ 2661.0[O3][SOJ + l.C
                                      Weibull model:
                                      Yield=531 x expKEOJ/0.133)] x exp[-([SO2]/0.892)]
                                      (Yield=g/m of row; [O3]:  ppm, seasonal 7 h/day mean; [SO2]: ppm, seasonal 4 h/day
                                      mean)
                                                                                                                Heagle et al.
                                                                                                                (1983)

-------
vfa
o
§
                    TABLE 5-9 (cont'd). SOME STATISTICAL MODELS OF COMBINED OZONE AND

                                          SULFUR DIOXIDE RESPONSES
Species
Amsoy-71 and
Corsoy-79 (pooled)
Tomato
New Yorker
Type of
Interaction
No
interaction


Model
Yield= 1934.4*exp[-([03]/0. 124)2'666]*exp[-([S02]/l .5 1 1)1 -044]
(Yield = kg/ha; [O3]: ppm, seasonal 7 h/day mean; [SO2]: ppm, seasonal 4 h/day mean)

Injury=-75.78 + 20.48m[PI]-29.16[O3]+l,016[O3]2+9.02tSO2]-17.29[SO2]2+258.76
[O3][SO2](PI=plastochron index, used as a covariate; [O3] and [SO2]: ppm)
Reference
Kress et al

Deveau et
(1987)a
. (1986)

al.
    aReport includes models for other growth variables.
8

-------
 1      was on top growth of pitch pine, in which NO2 reversed a growth stimulation caused by
 2      exposure to O3. In contrast, although Yang et al. (1982) also observed an antagonistic
 3      interaction on the  needle dry weights of two eastern white pine clones, in these cases NO2
 4      reversed the adverse effect of O3.
 5           There appear to have been only three studies using sequential exposures of O3 and
 6      NO2. Runecldes and Palmer (1987) exposed radish, wheat, bush bean and mint daily to
 7      0.08 to 0.1 ppm NO2 for 3 h (09:00 to 12:00) or to 0.08 to 0.1 ppm O3 for 6 h (12:00 to
 8      18:00), or to the two gases in sequence.  With each species except mint, pretreatment with
 9      NO2 significantly  modified the growth responses  to O3. In radish and wheat, the two gases
10      acted conjointly to reduce growth more than O3 alone, while in bean NO2 was antagonistic.
11      In studies with tomato,  Goodyear and Ormrod (1988) found that sequential exposure to
12      0.08 ppm O3 for 1 h followed by 0.21 ppm NO2 for 1 h significantly reduced growth.
13      No significant effects were found when the sequence was reversed or the two gases were
14     used as a mixture. However, since the study  did not include a treatment with O3 alone,
15      no information was obtained as to how NC^ may have influenced the response to O3.
16     Bender et al. (1991) exposed kidney beans in  open-top chambers in the field to the sequence:
17     O3 (08:00 to 16:00, ambient+0.50 ppm) followed by NO2 (16:00 to 08:00,
18     ambient+0.3 ppm), during two growing  seasons. No  significant treatment effects on growth
19     were observed in  1988, but in 1989 a significant interaction on total plant biomass was noted
20     after 48 days; the overnight NO2 exposures negated the inhibition caused by O3 with a
21      change from -32% to +14%, relative to  the controls.  This type of response is similar to that
22     observed on bean by Runeckles and Palmer (1987).
23          With such limited information, it is not possible to generalize, particularly since
24     antagonistic and additive responses have been reported even for individual species.
25     However, since on a daily basis changes  in NO2  levels tend to lead to maxima at times when
26     O3 levels are lowest, the evidence is sufficiently  compelling to indicate that modifications of
27     the O3 response as a result of increased NO2  are highly probable.
28
29     5.4.6.4  Hydrogen Fluoride and Other Gaseous Pollutants
30          The adverse effects of hydrogen fluoride, HF, released from the aluminum smelting
31     process and superphosphate fertilizer manufacture are well documented, but information

       December 1993                          5.9!      DRAFT-DO NOT QUOTE OR CITE

-------
 1     about possible HF/O3 interactions are limited to a single study. MacLean (1990) reported
 2     that exposures of corn plants on alternate days to 4 h at ljug/m3 fluorine as HF or 0.06 ppm
 3     O3 showed reduced rates of senescence, compared with plants exposed only to O3.
 4
 5     5.4.6.5   Acid Deposition
 6          The effects of acidic deposition have been extensively reviewed by Shriner et al.
 7     (1990).  Although concerns over the possible role of exposures to acid rain or acid fog and
 8     O3 in the forest decline syndrome led to several studies with forest tree species, studies have
 9     also been conducted on  crops.  Of over 80 recent reports of studies on over 30 species, more
10     than 75% of the reports indicated no significant interactions between O3 and acidity of
11     simulated acid rain (SAR) or acid fog. The reports are summarized in Table 5-10.
12     In 63 studies, there was either no effect of one or other of the pollutants  (usually acid rain)
13     or the effects of both pollutant stresses were simply additive.
14          However, in other studies, statistically significant interactions have been reported for
15     several species, as also  shown in Table 5-10.  For example, although a large number of
16     studies of loblolly pine revealed no interaction, Qiu et al.  (1992) reported significant
17     interactions on foliar and stem biomass with seedling trees of an O3-sensitive family.
18     However, since the study failed to show a significant main effect of acidity of the SAR, the
19     authors question whether the interaction is meaningful.
20          With Norway spruce, antagonistic interactions were  noted on stomatal conductance
21     (Barnes et al.,  1990a) and dark respiration (Barnes et al.,  1990b).  In contrast, Eamus and
22     Murray (1991) reported greater than additive effects of O3 and acid mist  on photosynthetic
23     rates.  However, no interactions were noted in nine other investigations (Table 5-10).
24          Kohut et al.  (1990) observed significant interactions  on needle and shoot growth of red
25     spruce.  In both cases the inhibition caused by O3 and  SAR at pH 5.1 was reversed by more
26     acidic rain at pH 3.1.  However, there were unexplained inconsistencies  in the trends since
27     the combination of intermediate O3 levels and low pH  resulted in the greatest reductions  in
28     dry matter.  Percy et al. (1992), also working with red spruce, observed  an unexplained
29     statistically significant interaction on the thickness of the needle epidermal cell cuticular
30     membrane:  at intermediate O3 exposures,  increased acidity led to reduced membrane
31     thickness while at lower or higher O3 levels led to thicker membranes.

       December 1993                           5-92       DRAFT-DO NOT QUOTE OR CITE

-------
    TABLE 5-10. REFERENCES TO REPORTS OF INTERACTION OR NO
     INTERACTION BETWEEN OZONE AND ACID RAIN OR ACID FOG
Species
Tree species:
CONIFERS:
Jeffrey pine
Loblolly pine
Ponderosa pine
Shortleaf pine
Slash pine
White pine
Douglas fir
Norway spruce
Red spruce
Sequoia
Totals
HARDWOODS:
Green ash
White ash
European beech
Paper birch
Sugar maple
Red oak
Yellow poplar
Totals
Crop species:
Interaction
No. References


0 —
1 41
0 —
1 52
2 9, 13
1 47
0 -
1 3, 4
2 31, 39
1 63
9

0 —
0 —
1 14
1 29
0 -
0
3 11, 12, 27
5

No.


1
13
2
1
0
3
1
9
5
0
35

1
1
1
0
2
2
1
8

No Interaction
References


62
1, 10, 16-21, 26, 32, 43, 47, 55
65,66
8
—
44, 46, 56
25
2, 5-7, 15, 24, 30, 36, 50
33, 34, 38, 40, 62
—


23
23
35
—
44,45
44,45
48


FORAGES AND FIELD CROPS:
Alfalfa
Sorghum
Soybean
Wheat
Totals
HORTICULTURAL CROPS:
Snap bean
Celery
Corn
Pepper
1 59
1 51
1 67
0 —
2

0 -
0 -
0 —
0 —
4
0
4
1
5

1
1
1
2
42, 53, 59, 64
—
28, 37, 53, 57
53


53
60
60
58,60
December 1993
5-93
DRAFT-DO NOT QUOTE OR CITE

-------
         TABLE 5-10 (cont'd). REFERENCES TO REPORTS OF INTERACTION OR NO
      	INTERACTION BETWEEN OZONE AND ACID RAIN OR ACID FOG	
                                         Interaction                  No Interaction
       Species                     No.    References           No.    References
       HORTICULTURAL CROPS (cont'd'):

       Strawberry                   0     —                   2     60, 61
       Tomato                      0     —                   2     53, 60
       Avocado                    1     22                   0     —
       Citrus                       1     22                   0     —
          Totals                    2                          9

       Others:

       Ivy                         0     -                   1     30
       Lichen (Lobaria)              0     —                   1     54
          Totals                    0                          2
       TOTALS:                   19                        63

      References:
      1. Adams and O'Neill (1991). 2. Barnes and Brown (1990). 3. Barnes et al. (1990a).  4. Barnes et al.
      (1990b).  5. Blank et al. (1990a).  6. Blank et al. (1990b).  7. Blaschke and Weiss (1990).  8. Boutton and
      Flagler (1990). 9. Byres et al. (1992). 10. Carter et al. (1992).  11. Chappelka et al. (1985).  12. Chappelka
      et al. (1988).  13. Dean and Johnson (1992).  14. Eamus and Murray (1991). 15. Ebel et al. (1990).
      16. Edwards and Kelly (1992). 17. Edwards et al. (1990).  18. Edwards et al. (1991).  19. Edwards et al.
      (1992). 20. Edwards et al. (1992). 21. Edwards et al. (1992).  22. Eissenstat et al. (1991). 23. Elliott et al.
      (1987). 24. Fuhrer et al. (1990).  25. Gorissen et al. (1991).  26. Hanson et al. (1988). 27. Jensen and Patton
      (1990). 28. Johnston and Shriner (1986).  29.  Keane and Manning (1988). 30. Kerfourn and Garrec (1992).
      31. Kohut et al. (1990).  32. Kress et al. (1988). 33. Laurence et al. (1989). 34. Lee et al. (1990).
      35. Leonard! and Langebartels (1990). 36. Magel et al. (1990). 37. Norby et al. (1986). 38. Patton et al.
      (1991). 39. Percy et al. (1992).  40. Pier et al. (1992). 41. Qiu et al. (1992). 42. Rebbeck and Brennan
      (1984). 43. Reddy et al. (1991). 44. Reich and Amundson (1985). 45. Reich et al. (1986). 46. Reich et al.
      (1987). 47. Reich et al. (1988).  48. Roberts (1990). 49. Sasek et al. (1991).  50. Senser (1990).  51. Shafer
      (1988). 52. Shelburne et al. (1993). 53. Shriner and Johnson (1987). 54. Sigal and Johnston (1986).
      55. Somerville et al. (1992).  56. Stroo et al. (1988). 57. Takemoto et al. (1987).  58. Takemoto et al.
      (1988a).  59. Takemoto et al. (1988b). 60. Takemoto et al. (1988c). 61. Takemoto et al. (1989). 62. Taylor
      et al. (1986).  63. Temple (1988). 64. Temple et al. (1987).  65. Temple et al.  (1992). 66. Temple et al.
      (1993).  67. Troiano et al. (1983).
1           Shelburne et al. (1993) reported that, in two growing seasons, needle biomass of
2      shortleaf pine was significantly reduced in tree seedlings receiving the highest O3 exposures
3      (2.5 x  ambient) and SAR at pH 3.3. However, there were no effects at lower O3 exposure
4      levels or higher pHs.
5           A three-year study of slash pine revealed a significant interaction on stem volume
6      increment  in each year  (Dean and Johnson,  1992).  This was attributed to a high rate of

       December 1993                             5-94       DRAFT-DO NOT QUOTE OR CITE

-------
 1     increase observed with increasing acidity in trees exposed to an intermediate O3 level
 2     (2 x ambient).  In contrast, at higher or lower O3 exposures, acidity of the SAR applied had
 3     little effect. Although another study with slash pine indicated a significant interaction on
 4     photosynthetic rates, no information was provided about its nature (Byres et al.,  1992).
 5          The mineral status (K, Ca and manganese, Mn) of white pine showed antagonistic
 6     interactions between O3 and SAR (Reich et al., 1988). Increased acidity nullified the
 7     increase in foliar K and the decreases in root CA caused by O3, while increased  O3 nullified
 8     the increase in root Mn that resulted from increased acidity.
 9          Temple (1988) reported a synergistic response of root growth of giant sequoia.  Yellow
10     poplar showed no interactions hi one study (Table 5-10), but a greater than additive response
11     of root growth was observed by Chappelka et al. (1985). Chappelka et al. (1988b) found
12     that although neither O3 nor the pH of SAR caused any significant main effects on growth, at
13     intermediate O3  levels increased acidity caused significant decreases in stem and  leaf
14     biomass.  Jensen and Patton (1990), on the other hand, reported significant antagonistic
15     interactions on yellow poplar leaf and shoot growth.  Based on estimates from growth models
16     derived from experimental data, increased acidity (pH 5.5 to pH 3.0) of SAR reduced the
17     decreases caused by O3 by almost 50%.
18           Adverse effects of O3 on the leaf area  and shoot, leaf, and root biomass of paper birch
19     were reversed by increased acidity  of SAR (Keane and Manning, 1988). Similarly, in both
20     avocado and lemon trees, Eissentstat et al. (1991) found that increased acidity  offset the
21     negative effects  of O3 on leaf growth.
22           Although there are four reports of no interactions on alfalfa, Takemoto et al. (1988b)
23     observed  significant interactions on leaf drop. In charcoal-filtered air,  leaf drop  increased by
24     a factor of six as the pH of the fog treatment changed from 7.24 to the extremely acid pH
25     1.68, the lowest level recorded in the field in southern California. In unfiltered  air, in
26     contrast, leaf drop only increased 20%.
27           Several studies with soybean revealed no significant interactions. However, Troiano
28     et al. (1983) reported a 42%  reduction in seed yield between charcoal-filtered  and unfiltered
29     air with SAR at pH 2.8, versus a 6% reduction at pH 4.0.  Increased acidity thus multiplied
30     the effect O3,  due largely to a stimulation of seed yield caused by increased acidity.  Shafer
31     (1988) observed a stimulation of shoot growth of sorghum at pH 2.5 of SAR over growth at

       December 1993                            5.95       DRAFT-DO NOT QUOTE OR  CITE

-------
 1     pH 5.5 as a result of which greater growth occurred at low O3 exposure levels, although
 2     there was no effect of acidity at the highest 03 level (0.3 ppm).
 3          In summary, although the majority of studies have not demonstrated the existence of
 4     interactions between O3 and SAR, where statistically significant interactions on growth or
 5     physiology have been reported, the interactions were mostly antagonistic. The only
 6     synergistic interactions reported are in two studies of yellow poplar and single studies of
 7     sequoia and shortleaf and slash pines. In most cases where significant interactions were
 8     noted, the authors have had difficulty in providing any mechanistic explanation.  It appears
 9     that, although the effects may have passed normally accepted  tests of statistical significance,
10     they may nevertheless have been  spurious findings. Overall,  it appears that exposure to
11     acidic precipitation is unlikely to  result in significant enhancement of the adverse effects of
12     O3 in most species.  In the few cases of antagonistic interactions, the suggestion was made
13     that these may have reflected a beneficial fertilizer effect due to the nitrate and sulphate
14     present in the SAR applied.
15
16     5.4.6.6   Heavy Metals
17           Interactions of O3 with several heavy metal pollutants were reviewed in the previous
18     criteria document (U.S. Environmental Protection Agency, 1986).  The limited data for
19     pollutants such as cadmium (Cd), nickel (Ni), and zinc (Zn) almost invariably showed that
20     they enhanced the adverse effects of O3, usually additively, but occasionally more than
21     additively.  To the results with Cd, Ni, and Zn on garden cress, lettuce, pea, tomato, and
22     aspen, reviewed at that time,  should be added similar findings with Zn on Pinto bean
23      (Mcllveen et al., 1975), with increased Zn resulting in significantly increased foliar injury
24      and decreased infection mycorrhizal establishment. However, in a study of the effects of Oj,
25      Ni, and copper (Cu) on tomato, Prokipcak and Ormrod (1986) found that as the levels of
26      both O3 and Ni increased, the interaction changed from additive to less than additive.
27      Complex interactions were observed when the treatments included both Ni and Cu.
28           No information appears to be available about possible interactions with lead. Although
 29     qualitatively heavy metals appear to increase plant sensitivity to O3, the limited information
 30     available precludes defining any  quantitative relationships.
 31

        December 1993                           5-96       DRAFT-DO NOT QUOTE OR CITE

-------
 1     5.4.6.7   Mixtures of Ozone with Two or More Pollutants
 2          Pollutant-pollutant interactions are not limited to mixtures or sequences of two
 3     pollutants.  Several studies have been made of interactions of O3 with various combinations
 4     of SO2,  NO2 and acid rain. However, in some of these investigations,  no treatment with
 5     O3 was included in the experimental design and therefore no information was  obtained on
 6     effects on the response to O3. Some studies using only repeated daily exposures to high
 7     levels (>0.3 ppm) of one or more pollutants are excluded from this review.
 8          Adaros et al. (1991b), hi a field study of spring rape using open-top chambers, found
 9     no significant interactions between O3 and NO2 (sequential exposures) and SO2 (continuous
10     exposures).  In a two-year study on spring barley and spring wheat, some statistically
11     significant interactions were noted but they were  scattered through the different growth
12     measurements, cultivars and years with no consistent pattern (Adaros et al., 1990a).
13     Additive effects with no interactions were observed in studies of shore juniper (Fravel et al.,
14     1984), radish (Reinert and Gray,  1981), and azalea (Sanders and Reinert, 1982).  Yang et al.
15     (1982) reported a less than additive interaction on injury to white pine.
16          No significant three-way interactions were found in studies of soybean (Norby et al.,
17     1985), yellow poplar (Chappelka et al.,  1985,  1988b), nor on other hardwood species (Davis
18     and Skelly, 1992; Jensen and Dochinger, 1989; Reich et al., 1985) exposed to O3, SO2 and
19     SAR.
20          No information was collected on interactions in the few published studies involving
21     03, SO2, NO2 and SAR.
22          The limited data make it difficult to draw any firm conclusions, but in general,  the
23     consequences of such exposures appear to be largely dictated by the dominant individual
24     two-way interaction.
25
26     5.4.7   Interactions with Agricultural  Chemicals
27          Agricultural chemicals are used for the control of insect pests, diseases,  and weeds, and
28     for the control of growth in specialized situations such as the selective  thinning of fruit on
29     orchard trees.  The potential for some agricultural chemicals to modify plant response to
30     O3, first noted with certain fungicides on Pinto beans (Kendrick,  1954), led to numerous
31     field and laboratory studies.  As noted in the previous criteria document (U.S. Environmental

       December 1993                          5.97      DRAFT-DO NOT QUOTE OR CITE

-------
 1     Protection Agency, 1986), protection against O3 injury was found to be conferred by
 2     applications of numerous commercial fungicides, herbicides and growth regulators.
 3          The available information is derived from studies involving a number of different
 4     commercial chemicals and species.  No comprehensive and systematic studies have been
 5     reported, but the weight of evidence indicates that certain fungicides are consistent in
 6     providing protection.  In particular, there have numerous reports of protection conferred by
 7     applications of benomyl (benlate; methyl-l-[butylcarbamoyl]-2-benzimidazolecarbamate).
 8     In addition to the studies reviewed  in the previous criteria document (U.S. Environmental
 9     Protection Agency,  1986), benomyl protection of grape (Musselman and Taschenberg,  1986)
10     and bean cultivars (Pell,  1976; Pellisier et al., 1972) has also been reported.  It is of interest
11     to note that although several nematocides were found to increase sensitivity of tobacco and
12     Pinto bean to O3, applications of benomyl overcame this response and conferred resistance
13     (Miller et al., 1976).  However, benomyl was found to increase the injury caused by PAN
14     (Pell and Gardner, 1979).  It should also be noted that many of the effective fungicides are
15     carbamates and have been used as  antioxidants in other applications such as  rubber
16     formulations.
17          The need to distinguish between protective action against O3 injury and fungicidal
18     activity per se is shown by a study of fentin hydroxide (Du-Ter; tetraphenyltin hydroxide) on
19     potato (Holley et al., 1985).  The fungicide reduced foliar injury in the field and also the
.20     colonization  of injured leaf tissue by the early blight fungus, Alternaria soktni.  However,
21     yield increases appeared to result from the reduction of disease rather than from diminished
22      O3 injury.
23           The triazoles are a family  of compounds with both fungicidal and plant growth
24      regulating properties.  Fletcher and Hofstra (1985) reported on the protective  action of
25      triadimefon (l-[4-chlorophenoxy]-3,3-dimethyl-l-[lH--l,2,4-triazo-l-yl]-2-butanone),and
26      Musselman and Taschenberg (1986) found that triadimefon and the triazole, etaconazole
27      (l-[[2,4-dichlorophenyl]-4-ethyl-l,3-dioxolan-2-yl]methyl-lH-l,2,4-triazole), were as
28      effective as benomyl in protecting grape from oxidant injury; cultivar differences were noted,
 29     with the fungicides being more  effective on Concord than on Ives foliage. Seed treatment
 30     with triazole S-3307 ([E]-l-[4-chlorophenoxy]-3,3-dunethyl-2-[l,2,4-triazol-l-yl]-
 31      l-penten-3-ol) resulted in a 50% reduction in the size of wheat plants but provided complete

        December 1993                           5-98       DRAFT-DO NOT QUOTE OR CITE

-------
 1     protection from an excessive  exposure to 0.5 ppm O3 for 6 h that resulted in severe necrosis
 2     on the leaves of untreated plants (Mackay et al., 1987).
 3          A range of commercial plant growth regulating compounds was studied by Cathey and
 4     Heggestad (1972).  The plant growth retardants, CBBP (Phosfon-D;
 5     2,4-dichloro-benzyltributyl phosphonium chloride) and SADH (Alar; succinic acid
 6     2,2-dimethyl-hydrazide) and several of its analogs, were found to be more effective than
 7     benomyl in reducing O3 injury on petunia.
 8          Conflicting reports of the effects of herbicide-O3 interactions were reviewed in the
 9     previous criteria document (U.S. Environmental Protection Agency, 1986).  Recent studies
10     of metolachlor (2-chloro-N-[2-ethyl-6-methlphenyl]-N-[2-methoxy-1 -methylethyl] acetamide);
11     Mersie et al., 1989) and atrazine (2-chloro-4-ethylamino-6-isopropylamino-.s-triazine); Mersie
12     et al., 1990) revealed species-dependent effects: metolachlor sensitized com to O3 but
13     offered protection to bean and soybean.  The effects of atrazine on corn were additive to
14     those induced by exposure to 0.2 ppm O3 for 6 h/day twice weekly for three weeks, but
15     antagonistic to exposures  to 0.3 ppm.  Mersie et al.  (1990) also observed a protective action
16     of the commercial  antioxidant, n-propyl gallate, on corn.
17          In spite of reports to the contrary (Teso et al.,  1979), Rebbeck and Brennan (1984)
18     found that the insecticide, diazinon (O,O-diethyl-O-[2-isopropyl-4-methyl-6-pyrimidinyl]
19     phosphorothioate), did not protect alfalfa from  O3 injury in a greenhouse  study.
20          Our knowledge of the interactions of these different types of agricultural chemical with
21     O3  is still too fragmentary to be able to draw any general conclusions other than to note the
22     general  efficacy of the carbamate fungicides.  As noted in the previous criteria document
23     (U.S. Environmental Protection Agency, 1986), it is premature to recommend their use
24     specifically for protecting crops from the adverse effects of 63, rather than for their primary
25     purpose.
26
27     5.4.8   Factors Associated with Global Climate Change
28          This section focuses solely on the ways in which features of global climate change may
29     be expected to affect the  impact of oxidants on vegetation. It is  not intended to provide a
30     comprehensive  review of the issues and components of climate change per se.
       December 1993                           5.99       DRAFT-DO NOT QUOTE OR CITE

-------
 1           The magnitudes and causes of some of the changes in features of the global climate that
 2      have beea observed or are predicted to occur are currently the subject of controversy.
 3      However,  there is clear evidence of increases in mean CO2 levels (Keeling et al., 1989)
 4      which together with other anthropogenic emissions of radiatively active gases may contribute
 5      to the upward trend in mean surface level temperatures observed over the past century
 6      (Jones, 1989) and changes precipitation patterns throughout the world (Diaz et al., 1989).
 7      In addition, depletion of the stratospheric O3 layer in the polar regions, caused by
 8      halofluorocarbons, results in increased penetration of the atmosphere by solar ultraviolet-B
 9      (UV-B) radiation (280 to 320 nm wavelengths). However, the intensity of UV-B radiation
10     reaching the earth's surface may be attenuated by O3-pollution in the lower troposphere
11      (Briihl and Crutzen, 1989).  Differences in  the degree of this attenuation probably contribute
12     to the discrepancies between recently observed trends in surface-level UV-B intensities
13     (Scotto et al., 1988; Blumenthaler and Ambach, 1990).
14          Independent of any effects of ambient temperature, CO2 level affects plant water
15     relations through effects on stomatal aperture and conductance, leading to effects on leaf and
16     canopy temperature and the uptake of gaseous pollutants. The effects of UV-B on numerous
17     growth processes have been reviewed by Tevini and Teramura (1989) and Runeckles and
18     Krupa (1993).  Individual interactive effects of O3 and several of these features of global
19     climate change have been reviewed in the previous sections.  However, it is important to
20     recognize that, because of the interactions among the different components of climate change
21     themselves, a holistic approach is essential, which includes their potential for modifying plant
22     response to oxidants.  Overall reviews of the interactions involving the factors of climate
23     change and O3 have been presented by Krupa and Kickert (1989) and Ashmore and Bell
24     (1991).
25           The effect of increased CO2 in stimulating photosynthetic rates may also lead to
26     increased leaf area, biomass and yield (Allen,  1990).  Increased CO2 also leads to stomatal
27     closure.  However, with regard to water use, the result of decreased stomatal conductance in
28     reducing  transpiration is partly offset by the increase in leaf and canopy temperature resulting
 29      from reduced evaporative cooling, and the  increase in leaf area.  The  net result is that
 30      increased CO2 may lead to only slight increases in water use efficiency that are attributable
 31      more to increased photosynthetic activity than to reduced transpiration (Allen, 1990).  On the

        December 1993                         5-100      DRAFT-DO NOT QUOTE OR CITE

-------
 1     other hand, since the primary route of entry into the leaf of a gaseous pollutant such as O3 is
 2     through the stomata, increased CO2 levels would be expected to decrease the impact of O3 by
 3     reducing uptake as a consequence of reduced stomatal conductance.
 4          Allen (1990) provides a simulation of the effect of doubling the average ambient CO2
 5     level from 340 to 680 ppm on soybean yield, based on the Weibull response model to 03 and
 6     SO2 of Heagle et al. (1983), and the model of stomatal conductance developed for soybean
 7     by Rogers et al. (1983):
 8
 9                     gg = 0.0485 - 7.00  x 10"5[CO2] + 3.40 x  10"8[CO2]2,
10
11     where gs is stomatal conductance (m/s), and [COJ is CO2 concentration (ppm).  According
12     to this model, a doubling of the CO2 level would reduce gs by  a factor of 0.69, effectively
13     reducing the O3 and SO2 concentrations to 0.038 and 0.018 ppm respectively. At the current
14     340 ppm CO2 level, the Weibull model predicts a yield of 340.5 g/m of row.  Reduced
15     pollutant entry at 380 ppm CO2 gives  a predicted yield of 390.6 g/m of row, an  increase of
16     14.7%.  This is a conservative estimate since it ignores the direct effect of the increased CO2
17     level on soybean growth.
18          Although the calculation makes numerous assumptions, it is qualitatively supported by
19     evidence from the few studies published to date on CO2/O3 interactions.  Barnes and
20     Pfirrmann (1992) reported that an increased CO2 level of 765 ppm countered the adverse
21     effects of O3 on photosynthesis, shoot growth rate, leaf area, and water use efficiency of
22     radish. Protection against the adverse effects of O3 on soybean by elevated CO2 was also
23     reported by Kramer et al. (1991). The yield loss due to O3 at  ambient CO2 was 11.9%,
24     whereas in the presence of ambient+150 ppm CO2, the loss was only 6.7%.
25          Although these studies support the prediction of Allen (1990), they were conducted in
26     growth chambers (Brown  and Pfirrmann,  1991) or open-top field chambers (Kramer et al.,
27     1991; Mulchi et al., 1992), as were the studies on which Allen's model was based.  Hence
28     the plants would not have been subjected to the environmental  conditions typical of the open
29     field, particularly with respect to wind speed and its effects on transpiration and  temperature.
30     Nevertheless they support the view that increased CO2 levels will reduce adverse effects of
31     O3 on crops.

       December 1993                          5-101      DRAFT-DO NOT QUOTE OR CITE

-------
 1          It is unclear as to whether such CO2-induced reductions of the impact of O3 also apply
 2     to the long term growth of trees, and it is equally unclear as to how increased CO^ will
 3     affect the impact of O3 on ecosystems.  These uncertainties arise because of the numerous
 4     compensatory feedback mechanisms that play important roles in both long-term perennial
 5     growth and in the behavior of ecosystems.  Such feedbacks include changing demands for
 6     nutrients, increased leaf area and potential water loss, and changes in litter quality and
 7     quantity. For example, in terms of the effects of increased CO^ alone, long-term studies of
 8     several species  suggest that although photosynthesis may be demonstrably stimulated, there
 9     may be little or no net response at the ecosystem level (Bazzaz, 1990).
10          The consequences of global warming as a  feature of climate change are difficult to
11     assess since, as discussed in Section 5.4.4,  the information on the effects of temperature on
12     O3-response is  conflicting.  However, as Ashmore and Bell (1991) point out, concerns over
13     the effects  of O3 on sensitivity to freezing temperatures will become increasing unimportant
14     as warming occurs.
15           Various models  of climate change scenarios have indicated that changed precipitation
16     patterns  will lead to increased drought in some mid-latitude regions of the world. The bulk
17     of the evidence reviewed in  Section 5.4.4 suggests that this would reduce the impact of 03.
18     However,  because of the major direct impact of drought per se, such protection  would be of
19     little practical significance.
20           Greater certainty surrounds the likelihood that global warming will increase the
21     incidence and severity of losses caused by pests and diseases.  Concurrent  increases may also
22     favor the competitiveness  of many weed species.  At present, it is not possible to quantify
23     such changes or to determine how they would influence the interactions discussed in
24     Section 5.4.3.
25           With regard to possible interactions of O3 and UV-B, Runeckles and Krupa (1993)
26     point out that,  because of the episodic nature of O3 pollution, including its typical diurnal
27     pattern,  surface level exposures to UV-B will also be episodic. They have described various
28     possible O3/UV-B scenarios that need to be considered.  With low surface O3 levels and
 29      increased  UV-B irradiation due to stratospheric O3 depletion, effects of UV-B will
 30      predominate.   On the other hand, elevated surface O3 levels will cause increased attenuation
 31      of UV-B resulting in reduced surface intensities. With no stratospheric 03 depletion, this

        December 1993                         5-102      DRAFT-DO NOT QUOTE OR CITE

-------
 1     condition implies that surface effects of O3 will predominate over the effects of the effects of
 2     UV-B; with stratospheric O3 depletion, the resulting surface level irradiation will be
 3     dependent upon the concentration and thickness of the surface O3 layer and both O3 and
 4     UV-B effects may occur.
 5          To date there have been no experiments conducted specifically to simulate these
 6     different scenarios.  However, Booker et al. (1992) exposed soybean in field open-top
 7     chambers within which lamps were suspended to provide increased intensities of UV-B.  The
 8     O3 treatments were ambient and 1.5 x ambient.  No significant O3/UV-B interactions were
 9     noted; the effects on growth were solely attributable to the O3 exposure.  However, increased
10     UV-B irradiation resulted hi increases in the foliar content of UV-absorbing constituents.
11     In contrast, Miller and Pursley (1990) reported that a preliminary experiment revealed a less
12     than additive interaction of O3 and UV-B on soybean growth.
13          It is clear overall that the effects of O3 on vegetation will be modified to some degree
14     by various components of the complex mix of factors that constitute climate change.
15     Considerably more research will need to be undertaken before quantitative assessments of the
16     magnitudes of the changes will be possible.
17
18     5.4.9   Summary
19          Since the previous criteria document (U.S.  Environmental Protection Agency, 1986),
20     additional studies have been published on a wide range  of biological, physical, and chemical
21     factors in the environment that interact with plant response to O3.
22          Biological components of the environment of individual plants include pests, pathogens
23     and plants of the same or other species in competition.  With regard to insect pests, although
24     only a very limited number  of plant-insect systems has been studied, there is a general trend
25     in the observations that suggests that some pests  have a preference for and  grow better when
26     feeding on plants that  have been impacted by O3. Unfortunately, because we have no
27     knowledge of how the vast majority plant-insect  systems will be affected by O^, it is not
28     possible to offer any quantitative overall assessment of the consequences  of such interactions
29     on the growth of crops and  natural vegetation. At best, we may conclude that there is a
30     reasonable likelihood that some insect pest problems will increase as a result of increased
31     ambient O3 levels, but there is no evidence to suggest that O3 may trigger pest outbreaks.

       December 1993                          5-103      DRAFT-DO NOT  QUOTE OR CITE

-------
 1          Plant-pathogen systems are also affected by O3 but here too, the available evidence is
 2     far from representative of the wide spectrum of plant diseases.  Nevertheless, the suggestion
 3     of Dowding (1988) that diseases caused by obligate pathogens tend to be diminished by
 4     O3 while those caused by facultative pathogens tend to be favored, is generally supported by
 5     the limited evidence available.  In terms of its broader implications, this suggests that
 6     continued exposure to O3 may lead to a change in the overall pattern of the incidence and
 7     severity of specific plant diseases affecting crops and forest trees.  However, it is not
 8     possible  with the limited evidence currently available to predict whether the net consequences
 9     would be more harmful or less.
10          A major level of uncertainty concerns the effects of O3 at the population and
11     community levels within natural ecosystems. Very few studies have been conducted on
12     multi-species systems, and Woodward  (1992) has pointed out the hazards of attempting to
13     extrapolate from responses of the individual plant to responses of a population of such plants.
14     This is borne out by the observations of Evans and Ashmore (1992) who showed that the
15     behavior to O3-exposure of a species growing in mixture with other species  is not predictable
16     from its behavior when grown in isolation.  This has serious implications with regard to
17     complex natural ecosystems, and identifies a serious gap in our knowledge of the effects of
18     O3 that can only be filled by a substantial research  effort.
19           With regard to the physical environment, the  combination of light, temperature and
20     water availability largely determines the success of plant growth because of the influence of
21     these factors on the processes of photosynthesis, respiration and transpiration.  For
22     agricultural crops, perhaps the most important of these potential interactions with
23     O3 concerns water availability and use. There is consistent evidence that drought conditions
24     tend to reduce the direct adverse effects of O3 on growth and yield.  Conversely, the ready
25     availability of soil water tends to increase the susceptibility of plants to O3 injury.  However,
26     a lack of water should not be viewed as a potentially protective condition, because  of the
27     adverse effects of drought per se. The combination of drought conditions and exposure to
28      O3 is likely to result hi  adverse effects on growth and yield that are largely the result of lack
29      of water.  However, with perennial trees,  there is evidence that prolonged exposures to
30      O3 may lead to greater water use efficiency which would enable such trees to be better able
31      to survive drought conditions.

        December 1993                           5-104       DRAFT-DO NOT QUOTE OR CITE

-------
 1           In contrast with crop species, with tree species the relative roles of light, temperature
 2      and water are shifted somewhat because of the differences in plant form.  In particular, the
 3      photosynthetic function of the leaves is carried out by a much smaller proportion of the
 4      plant's biomass.  Conversely, a larger demand is placed on temperature-dependent
 5      respiratory processes to maintain and support the tissues of the stem and root systems.
 6      In addition, in temperate regions, the perennial habit brings with it the requirement for
 7      storage of carbohydrates and other reserves, in order to permit survival during the winter
 8      season and to facilitate renewed spring growth. Hence,  with tree species it becomes
 9      important to distinguish between the immediate effects of exposure to 03 and the longer-term
10      consequences of these effects.
11           Of particular importance in northern latitudes and at higher elevations is the
12      demonstrated role of O3 in adversely affecting cold hardiness, by reducing carbohydrate
13      storage.  Independent of effects on winter hardiness,  there is also evidence to indicate that
14     adverse effects on storage may also be a component of changes in growth occurring in
15      subsequent seasons (Hogsett et al., 1989; Anderson et al., 1991; Sasek et al., 1991).
16     However, it is not yet possible to assemble these observations into a general quantitative
17     model.
18          The plant's environment also contains numerous chemical components, ranging from
19     soil nutrients and other air pollutants to agricultural chemicals used for pest, disease and
20     weed control.  With regards to plant nutrients and their influence on plant response to
21      O3, the available evidence is highly  fragmentary and frequently contradictory, and hence
22     does not permit the drawing of any general conclusions.  A large number of studies have
23     been conducted on the effects of O3  in conjunction with other gaseous air pollutants such as
24     SO2 and NO2, although the information obtained in several of the studies is of no  more than
25     academic interest because of the unrealistic exposure conditions used.  Although there is
26     clear evidence to show that O3 and SO2 may act synergistically in increasing foliar injury in
27     some species,  the available evidence indicates that this type of response is not universal.
28     Several empirical models of the O3-SO2 interaction have been developed, but they have little
29     in common and are highly specific to the crop and exposure conditions used.  Furthermore,
30     the frequently observed lack of interaction implies that in many cases the impact of 03 is
       December 1993                           5_105     DRAFT-DO NOT QUOTE OR CITE

-------
 1     probably best assessed on its own.  The same is true of the situation with regard to
 2     combinations of O3 and acid rain or acid fog, and O3 and NO2.
 3          Numerous agricultural chemicals have been found to influence the responses of plants
 4     to O3.  In particular, several fungicides have been shown to confer protection against visible
 5     injury, although none has been adopted for commercial application for this purpose.  On the
 6     other hand, the experimental chemical, ethylenediurea, has been found consistently to
 7     provide protection of a wide range of species, both in the laboratory and in the field.
 8          Since increased tropospheric O3 is a component of global climate change, results from
 9     studies on the interactions of O3 with increased levels of CO2 and UV-B radiation are
10     beginning to appear. Initial work with CO2 suggests that increased CO2 levels may
11     ameliorate the effects of O3.  However, it is too soon to be able to generalize on the outcome
12     of this interaction.  At the present time, no investigations of the compound interactions
13     involving O3, CO2, UV-B, increased temperature and changed soil moisture status have been
14     reported.
15          In conclusion, in spite of the amount of work carried out to date on the interactions of
16     O3 with environmental factors, we are left with a very fragmented understanding from which
17     to draw conclusions.  This is probably inevitable in view of the  vast scope of the possible
18     interactions between O3 and all the other environmental variables. It is  also a result of the
19     fact  that most of the published work consists of studies resulting from personal interests of
20     the investigators, rather than  from coordinated programs of research that focus on systematic
21     investigations.
22
23
24     5.5    EFFECTS-BASED AIR QUALITY EXPOSURE INDICES
25     5.5.1   Introduction
26     5.5.1.1  Biological Support for Identifying Relevant Exposure Indices
27           The effects of O3 on individual plants and factors that modify plant response to O3 are
28     complex and vary with species, environmental conditions, and soil and  nutrient conditions.
29     Because  of the complex effect of Oj and its interactions with physical and genetic factors that
30     influence response, the development of exposure indices to characterize plant exposure and to
31     quantify the relationship between O3 exposure and ensuing plant response has been and

       December 1993                         5-106      DRAFT-DO NOT QUOTE OR CITE

-------
 1     continues to be a major problem.  At best, experimental evidence of O3's effect on biomass
 2     production can refine our knowledge of those factors of O3 exposure that affect our ability to
 3     predict plant response using exposure indices.  The impacts of measured O3 concentrations
 4     on plant response are discussed and evaluated to determine the key factors of exposure that
 5     account for the variations in plant response and, if possible, to develop measures of pollutant
 6     exposure which relate well with plant response.
 7           Considerable evidence of the primary mode of action of 63 on plants (e.g., injury to
 8     proteins and membranes,  reduction in photosynthesis, changes in allocation of carbohydrate,
 9     and early senescence), which eventually impacts biomass production, identifies O3 uptake as
10     the correct characterization of plant exposure (Section 5.3).  Ozone uptake is controlled by
11     canopy conductance,  stomatal conductance, and ambient O3 outside the leaf (see Figure 5-3).
12     Any factor that will affect stomatal conductance (e.g., light, temperature, humidity, soil and
13     atmospheric chemistry and nutrients, time of day, phenology, and biological agents) will
14     affect O3 uptake and, consequently plant response (i.e., yield or biomass).  Biochemical
15     mechanisms describe  the mode of action of O3 on plants as the culmination of a series of
16     physical, biochemical, and physiological events leading to alterations in plant metabolism.
17     Ozone-induced injury is cumulative,  resulting in net reductions in photosynthesis, changes in
18     allocation of carbohydrate, and early senescence, which ultimately lead to reductions in
19     biomass production.  In most cases, increasing the duration of exposure increases the effect
20     of O3 on plant response.  Peak concentrations occurring during daylight when stomatal
21     conductance is high have  more influence in determining the impact of O3 on plant response
22     than lower concentrations or night concentrations because of a greater likelihood of
23     intracellular impairment.
24           From a lexicological perspective, duration and peak concentrations above some level
25     have value in determining plant response but interact with other factors such as  respite time,
26     temporal variation,  phenology, canopy structure, physiological processes, environmental
27     conditions, and soil and nutrient conditions in different fashions, depending upon species.
28     Effects occur on vegetation when the amount of pollutant absorbed exceeds the ability of the
29     plant to detoxify O3 or repair the initial impact  (Tingey and Taylor, 1982).
30          Although O3 uptake integrates the above factors with atmospheric conditions and relates
31     well with plant response,  it is  difficult to measure.  Several empirical models to predict

       December 1993                          5407     DRAFT-DO NOT QUOTE OR CITE

-------
 1     stomatal conductance have been developed for particular species (Losch and Tenhunen, 1981)
 2     but have not been used to estimate O3 uptake or to develop exposure indices.
 3
 4     5.5.1.2  Historical Perspective on Developing Exposure Indices
 5          For almost seventy years, air pollution specialists have explored alternative
 6     mathematical approaches for summarizing ambient air quality information in biologically
 7     meaningful forms that can serve as  surrogates for dose for vegetation effects purposes. Some
 8     of the indices introduced have attempted to incorporate some of the factors (directly or
 9     indirectly) described above.  Recognizing the importance of duration and peak concentrations
10     in conjunction with stomatal conductance, the optimum exposure index can be written as:
11
12                                    Index = Ei=1na Wj x f(Cj)                          (5-1)
13
14     where  Q is the hourly mean concentration, f(C{) is some function of Q, and Wj is some
15     weighting scheme that relates ambient condition and internal O3 flux. The optimal weights
16     are difficult to develop because of the complex relationship among exposure, environmental
17     condition, and species.
18          Equation (5-1) represents a taxonomy of exposure indices that have been proposed as
19     surrogates of dose in the literature. The exposure indices  differ in the ways in which the
20     values are assigned to Wj. Based on the weighting function, the exposure indices can be
21     arranged into the following categories (description from Lee et al., 1989):
22
23            •  One Event: Wj=0 for all CA except for the few  concentrations where Wj=l.
24               Examples of such indices are the second highest daily maximum 1-h
25               concentration  (2ndHDM), the maximum of 7-h (P7) and 1-h (PI) maximum
26               daily averages, and the 90th or higher percentiles of hourly distribution;
27
28            •  Mean:  w—0 for all CA outside the period of interest, P, and wi=vi/'Ei=ini
29               Vj for all Cj inside the period P where VA is a function of CA or some
30               environmental variable.  Examples are the seasonal mean of 7-h daily
31               means (M7) (Heagle et al., 1979); the effective mean, denoted me, where
32               mev is the index in Equation (5-1)  with f(Cj)= Ci"1/v  and w—1 for some
33               parameter v (Larsen and Heck, 1984); the solar-weighted mean where vt is
34               the hourly solar radiation value (Rawlings et al., 1988);
35

        December 1993                          5-108      DRAFT-DO NOT QUOTE OR CITE

-------
 1            •  Cumulative:  w—1 for all C{.  An example is the seasonal sum of hourly
 2               concentrations (i.e., total exposure, denoted as SUMOO);
 3
 4            •  Concentration Weighting:  w^gCC;) where g() is a monotonically non-
 5               decreasing function.  Examples are the seasonal sum of hourly
 6               concentrations at or above a threshold level such as 0.06 ppm (SUM06) or
 7               0.08 ppm (SUM08); the seasonal sum of the difference between an hourly
 8               concentration above a threshold level less the threshold value, such as
 9               0.08 ppm (AOT08);  the total impact with w—C/"1"17^ for some v (Larsen
10               et al., 1983); the index with the allometric function, g(Ci)=Cia, a>0; the
11               index with sigmoidal weighting function, g(Ci) = l/[l+M x exp(-AxCi)],
12               where M=4,403 and A=126, denoted as W126 by Lefohn et al. (1988a),
13               and M=500 and A=100, denoted SIGMOID by Lee et al.  (1989);  total
14               hours with concentrations at or above a threshold level, such as 0.08 ppm
15               (HRS08), g(Ci)=0 for Cj<0.08 ppm and w^l/Q for Cj>0.08 ppm;
16
17           •  Multicomponent:  wi=g(Ci, i).  Examples are indices that incorporate
18              several characteristics of exposure and crop development stage, including
19              the phenologically weighted cumulative impact indices (Lee et al., 1987).
20
21
22          Oshima (1975) and Oshima et al. (1976) proposed an exposure index, where the

23     difference between the value above 0.10 ppm and 0.10 was summed. This is referred to as

24     the AOT10 exposure index with f(C£)=CrO. 10 and w£=0 for C{ < 0.10 ppm and wt= 1 for
25     Cj^O.10 ppm in Equation (5-1).  Alternatively, Lefohn and Benedict (1982) introduced an

26     exposure index based on the hypothesis that if the higher O3 concentrations had greater value

27     in predicting adverse effects on agricultural crops than the lower values, then the higher

28     hourly mean concentrations should be given more weight than the lower values.  This index
29     summed all hourly concentrations equal to and above a 0.10 ppm threshold level. This index
30     is referred to as the SUM10 exposure index with f(Cj)=Cj and W;=0 for C^O.10 ppm and
31     wj=l for Cj^O.10 ppm.

32          A 6-h long-term seasonal mean O3  exposure index was used by Heagle et al. (1974).
33     Also, Heagle et al. (1979) reported the use of a 7-h experimental period mean. The 7-h

34     (0900 to  1559 h) mean, calculated over an experimental period,  was adopted as the statistic

35     of choice by the U.S. EPA's NCLAN program (Heck et al., 1982).  The 7-h daily daylight
36     period was selected by NCLAN because the index was believed to correspond to the period
37     of greatest plant susceptibility  to O3 pollution.  In addition, the 7-h period of each day
38     (0900 to  1559 h) was assumed to correspond to the time that the highest hourly


       December 1993                          5-109      DRAFT-DO NOT QUOTE OR CITE

-------
 1      O3 concentrations would occur. However, not all monitoring sites in the United States
 2      experience their highest O3 exposures within the 0900 to 1559 h 7-h time period (Lefohn and
 3      Jones, 1986; Lefohn and Irving, 1988; Logan, 1989).  Toward the end of the program,
 4      NCLAN redesigned its experimental protocol and applied proportional additions of O3 to its
 5      crops for 12-h periods. The expanded 12-h window reflected NCLAN's desire to  capture
 6      more of the daily O3 exposure.  In the published literature, the majority of NCLAN's
 7      experiments were summarized using the 7-h experimental-period average.
 8          As additional evidence began to mount that higher concentrations of O3 should be given
 9      more weight than lower concentrations (summarized in U.S. Environmental Protection
10      Agency, 1986), concerns about the use of a long-term average to summarize exposures of
11      O3 began appearing in the literature  (Lefohn and Benedict, 1982; Tingey, 1984; Lefohn,
12      1984;  Lefohn and Tingey, 1985; Smith et al., 1987). Specific concerns were focused on the
13      fact that the use of a long-term average failed to consider the impact of peak concentrations.
14      The 7-h seasonal mean contained all hourly concentrations between 0900 to 1559 h; this
15      long-term average treated all concentrations within the fixed window in a similar manner.
16      A large number of hourly distributions within the 0900 to 1559 h window could be used to
17      generate the same 7-h seasonal mean, ranging from those containing many peaks to those
18     containing none. Larsen and Heck (1984) pointed  out that it was possible for two air
19     sampling sites with the same daytime arithmetic mean O3 concentration to experience
20     different estimated crop reductions.
21           In the late 1980s, the focus of attention turned from the use of long-term seasonal
22     means to cumulative indices (i.e., exposure indices that sum  the products of concentrations
23     multiplied by time over an exposure period). As indicated previously, the cumulative index
24     parameters proposed by Oshima (1975) and Lefohn and Benedict (1982) were similar.  Both
25     parameters gave equal weight to the higher hourly  concentrations, but ignored the
26     concentrations below a subjectively defined minimum threshold (e.g., 0.10 ppm).  Besides
27     the cumulative indices proposed by Oshima (1975), Oshima et al. (1976), and Lefohn and
28     Benedict (1982), other cumulative indices were suggested,  including (1) the number of
29     occurrences of daily maximum hourly averaged concentrations greater than a threshold level
30     (Ashmore, 1984) and (2) the use of exponential functions (Nouchi and Aoki, 1979; Larsen
31     and Heck, 1984) to assign unequal weighting to O3 concentrations.

       December 1993                         5-110      DRAFT-DO NOT QUOTE OR CITE

-------
 1           A possible disadvantage of applying an integrated exposure index, as defined by
 2      Oshima (1975) or Lefohn and Benedict (1982), is that the use of an artificial threshold
 3      concentration as a cutoff point eliminates any possible contribution of the lower
 4      concentrations to vegetation effects.  Although this disadvantage may not be important when
 5      considering O3 exposures that occur in the California South Coast Air Basin, where repeated
 6      high concentrations are experienced from day-to-day and there are relatively short periods
 7      between episodes, it is important when assessing the typical exposures experienced in other
 8      parts of the United States.
 9           Recognizing the disadvantage, Lefohn and Runeckles (1987) suggested a modification to
10      the Lefohn and Benedict (1982) exposure index by weighting individual hourly mean
11      concentrations of O3 and summing over time. Lefohn and Runeckles (1987) proposed a
12      sigmoidal weighting function that was used in developing a cumulative integrated exposure
13      index.  The index included the lower, less biologically effective concentrations in the
14     integrated exposure summation.
15           None of the exposure indices mentioned above fully characterize the potential for plant
16     uptake of O3 because the indices, being measures of ambient condition, ignore the biological
17     processes controlling the transfer of O3 from the atmosphere through the leaf and  into the
18     leaf interior (U.S. Environmental Protection Agency,  1986, 1992).   Early studies with beans
19     and tobacco, reviewed in the previous criteria document (U.S. Environmental Protection
20     Agency, 1986), showed that short-term higher-peak exposures induced more injury than
21     longer-term  lower-peak exposures of the same total exposure, indicating that concentration
22     has more value than exposure duration in eliciting a response. Other studies with soybean,
23     tobacco, and bean, conducted prior to 1983 and described in U.S. EPA (1986),  showed that
24     the foliar injury response to subsequent peak exposures  varies with temporal pattern.
25     Predisposition to low levels of O3 for a few days increases plant sensitivity to subsequent
26     peaks (Johnston and Heagle, 1982; Heagle and Heck, 1974; and Runeckles and  Rosen,
27     1977).  Tobacco plants exposed to two consecutive days of peak exposures  showed greater
28     injury on the first day (Mukammal, 1965).  Plants exposed to a series of successive short
29     exposures suffered more injury than did those plants that received a continuous uniform
30     exposure, with all plants receiving equal total exposure  (Stan and Schicker, 1982).
       December 1993                          5411      DRAFT-DO NOT QUOTE OR CITE

-------
 1          When yield or growth are considered, "not only are concentration and time important
 2     but the dynamics of the O3 exposure are also important" (U.S. Environmental Protection
 3     Agency,  1986).  Musselman et al.  (1983) and Hogsett et al. (1985a) were among the first to
 4     demonstrate that plants exposed to  variable concentrations showed greater effect on plant
 5     growth than those exposed to a fixed or daily peak concentration of equal total exposure but
 6     lower peak concentrations. Musselman et al. (1986), in a subsequent experiment, exposed
 7     kidney bean plants to either a simulated ambient or a uniform concentration that had equal
 8     total exposure and peak concentration (at two levels of 0.30 and 0.40 ppm) and found that
 9     the effects of the two distributions  did not differ significantly.  Consequently, when peak
10     concentrations and total exposures  are equal, the diurnal distribution of concentrations
11     appears to be unimportant.
12          More recent studies with bean (Kohut et al.,  1988), soybean (Heagle et al., 1986), and
13     tobacco (Heagle et al., 1987) (reviewed in U.S. Environmental Protection Agency, 1992)
14     showed conflicting evidence of no  significant differences in response to different exposure
15     patterns of equal total exposure but varying peak concentrations.  The value of peak
16     concentrations in influencing response is inconclusive in these  studies because of low
17     statistical power. For the study with beans, plants exposed to  peak exposures  showed
18     significant impairment in the early harvests, but at the final harvest, O3 effects on growth
19     and yield were not statistically significant.  For the NCLAN studies with soybean and
20     tobacco, differences in yield between the constant and proportional 7-h O3 addition exposures
21     were not significant, even though the proportional-addition treatments had greater peak
22     concentrations.  In reanalysis of the soybean and tobacco studies, Rawlings et  al.  (1988)
23     stated that the differences between the constant and proportional O3 additions were relatively
24     small, thus  limiting the power of the comparison test.  However, 12-h exposures caused
25     greater effects than 7-h exposures  but the decrease in yield loss was not directly proportional
26     to the increased length of exposure (Rawlings et al., 1988).
27           Considerable research since the publication of the previous criteria document (U.S.
28     Environmental Protection Agency, 1986) has been directed at  developing measures of
29      exposure that were consistent with then-current knowledge of  the mode of action of 63 on
30      plants and on factors including concentration,  duration, and temporal dynamics of exposure
 31      influencing response.  A number of retrospective studies of existing data to evaluate and

        December 1993                          5-112      DRAFT-DO NOT QUOTE OR CITE

-------
 1     compare exposure indices based on statistical fit have been summarized in the literature
 2     between 1986 and 1988 and reviewed by the U.S. EPA (1992) (Rawlings et al., 1988;
 3     Adomait et al., 1987; Cure et al., 1986; McCool et al.,  1986,  1987; Smith et al., 1987; Lee
 4     et al., 1987, 1988; Lefohn et al., 1988a; Tingey et al., 1989; Musselman et al., 1988).
 5     These studies support the conclusion that: (1) O3 effects are cumulative; (2) peak
 6     concentrations are more important than lower concentrations in eliciting a response; and
 7     (3) plant sensitivity to O3 varies with time of day  and crop development stage. Exposure
 8     indices that cumulate the exposure and preferentially weight the peaks yield better statistical
 9     fits to response than the mean and peak indices.
10          Because the mean exposure index treats all concentrations equally and does not
11     specifically include an exposure duration component, the use of a mean exposure index for
12     characterizing plant exposures appears to be inappropriate for relating exposure with
13     vegetation effects (U.S. Environmental Protection Agency, 1992).  In particular, the
14     weighting of the hourly O3 concentrations of the mean is inconsistent with the weighting
15     function of plant exposure to O3 in Equation (5-1), which attempts to relate 03 flux with
16     ambient condition. The total exposure index includes an exposure  duration  component but
17     does not adequately relate pollutant exposure with plant response because the index weights
18     all concentrations equally and focuses on the lower concentrations, whose impact on
19     vegetation is minimal.
20          Evidence supporting the use of peak-weighted, cumulative indices in relating
21     O3  exposure and plant response is growing.  However, it is unlikely that the empirical
22     modeling of plant response will determine the optimal weighting function of hourly
23     O3  concentrations for use in characterizing plant exposure, which vary with environmental
24     factors and species. The development and comparison of exposure indices based on
25     statistical fits is difficult because only a limited number of experiments have been specifically
26     designed to  test and evaluate the various exposure indices.
27          While much research has been conducted on O3 effects on crops and trees between
28     1988 and the current period, our overall understanding of the mode of action of C^ on plants
29     and factors that modify plant response remains unchanged since the previous criteria
30     document (U.S. Environmental Protection Agency,  1986) and its supplement (U.S.
31     Environmental Protection Agency, 1992).  Additional studies further  support the value of

       December 1993                           5-113     DRAFT-DO  NOT QUOTE OR CITE

-------
 1      concentration, duration, and temporal pattern of exposure in describing plant exposure and its
 2      relation to plant response. Studies that applied two or more different exposure patterns of
 3      equal exposure but possibly different peak concentrations are reviewed in Section 5.5.2.2 to
 4      substantiate the value of exposure structure in influencing the magnitude of plant response.
 5      Recent papers that report results from replicate studies over time and/or space are
 6      summarized in Section 5.5.2.3 to test the value of duration and its relation with plant
 7      response.  In addition, a  few recent studies that provide additional insight to those factors
 8      that modify plant response are reviewed in Section 5.5.2.4.
 9
10     5.5.2    Developing Exposure Indices
11      5.5.2.1   Experimental  Design and Statistical Analysis
12          Controlled and field exposure-response studies, where extraneous  factors influencing
13     response are controlled or monitored, allow one to study concentration,  duration, respite
14     time, temporal fluctuations at general and specific stages of crop development in influencing
15     response. These studies provide insight on the efficacy of exposure indices in explaining
16     variation of response.  A small number of experiments have been designed specifically to
17     study the components of exposure and have applied two or more different patterns of
18     exposure which measure the same SUMOO values.  These designs provide the best evidence
 19     to determine whether plants respond differentially to temporal variations in
20     O3 concentrations. However, they  may have limited application in developing a statistical
21     relationship between O3  exposure and plant response.  Other design considerations,  including
22     the number, kind, and levels of O3 exposure, the patterns of randomization, the number of
 23      replicates used in the experiment, and experimental protocol, determine the (1) strength of
 24      the  statistical analysis that is applied to the treatment mean comparison tests and (2) range of
 25      ambient and environmental conditions over which generalizations may  be made.   These
 26     designs have been successfully used to test the value of components of exposure, particularly
 27     concentration, in influencing response (Musselman et al., 1983, 1986;  Hogsett et al., 1985a).
 28     Different approaches that include either a mean separation procedure and/or a regression
 29     procedure have been used to identify those important components of exposure that influence
 30     response.


        December 1993                          5-114     DRAFT-DO NOT QUOTE OR  CITE

-------
 1          To identify the importance of exposure in contributing to variation of plant response,
 2     the majority of pollutant effects studies use regression-based designs that apply a single
 3     pattern of exposure at varying concentration levels.  However, using these designs, the
 4     application of the results is limited; the order of plant response (i.e., plant yield) with respect
 5     to exposure is unchanged with different measures of exposure. The relative position and
 6     spacing between exposure levels is a function of how the exposure index weights the hourly
 7     03 concentrations and governs the statistical fit to response.  The regression approach has
 8     been used to compare and evaluate various exposure indices but the ability to discriminate
 9     among indices is low for these studies. By their nature, those studies that have used
10     regression-based designs that utilize data from single patterns  of exposure cannot distinguish
11     between mean exposure indices and sums constructed from means (i.e., mean x duration)
12     and, consequently cannot be used to test the value of duration in explaining the variation of
13     response.
14          Evidence to substantiate the value of duration in explaining the experimental variation
15     of plant response may be obtained when combining data from replicate studies of the same
16     species and cultivar over time and/or space. Pooling of data from replicate studies of the
17     same species to evaluate duration effects and/or to compare various  exposure  indices assumes
18     that the primary cause of biological response is pollutant exposure.  This assumption may or
19     may not be valid, particularly when plants from replicate studies are grown under varying
20     environmental, edaphic, and/or agronomic conditions that tend to mask the treatment  effects
21     during the growth of the plant (Section 5.3).  Hence, it is more difficult to substantiate the
22     importance of exposure-dynamic factors from retrospective analyses of combined data from
23     replicate studies of  the same  species than from experiments designed specifically to address
24     the components of exposure.  The comparison of environmental conditions, as well as the
25     yields  of plants exposed to charcoal-filtered air over replicate studies, is a simple check of
26     interaction but does not ensure that O3 effects on response can be isolated. In addition, when
27     the main effect of O3 is insignificant, the data may be limited for determining the  value of
28     duration or other components of exposure in predicting response.  Nonetheless, if an  air
29     pollutant is the primary source of variability in plant response, the relationship between
30     exposure and response should be consistent when data sets for the same crop are combined
31     over several years and/or locations.

       December  1993                          5_H5      DRAFT-DO NOT QUOTE OR CITE

-------
 1          Sets of replicate studies of equal and varying duration are readily available in the
 2     published literature but only a few reports have combined the data to specifically test the
 3     value of duration in explaining variation of plant response or to evaluate exposure indices
 4     based on statistical fit. Lefohn et al. (1988a) were the first to fit a common response model
 5     to combined data from two replicate studies of varying duration using various exposure
 6     indices.  Greater yield losses occurred when plants were exposed for the longer duration,
 7     indicating that the duration component of exposure was important in influencing response and
 8     that a cumulative-type index was able to describe adequately the  relationship between
 9     exposure and yield.  More recent papers have reported results of the two years  of replicate
10     studies and a few papers have used the regression approach with and without variance
11     components for sites and/or years to evaluate various exposure indices based on the adequacy
12     of fit of a common response model.
13          A number of the papers  relevant to the study of components of exposure influencing
14     plant response report only the mean and total exposure (i.e., sum of all hourly average
15     concentrations—SUMOO) indices.  Because exposure indices weight hourly 03 concentrations
16     differently,  it is almost impossible to transform one index into another.  One must return to
17     the original data, which in many cases are not available,  to generate alternative exposure
18     indices.  Therefore,  unless adequate information is given to allow calculation of exposure
19     indices, the analysis of reported results from individual and combined data to evaluate
20     different exposure indices is not possible,  although it may be possible to perform
21     retrospective evaluation of the structure of exposure in altering plant response.
22           Another concern relates to the experimental design, particularly the number,  kind, and
23     levels of exposure used in the study.  Generalization of experimental results is largely
24     dependent on the degree to which atmospheric and biospheric conditions mimic those of the
25     target population. However desirable the need to mimic the real world, understanding the
26     relationship between exposure and the ensuing response (i.e.,  plant yield) and to identify
27     those components of exposure in influencing response may require the use of exposure
28      regimes with temporal pattern, concentration, and/or structure that are not observed in
29      nature.  Research goals are difficult to attain when the investigator requires exposure levels
30      between  charcoal-filtered and near-ambient conditions, but the mathematician who is
        December 1993                          5-116      DRAFT-DO NOT QUOTE OR CITE

-------
 1     modeling the experiment requires higher than ambient levels of O3 to better describe the
 2     nature of plant response to O3.
 3          For example, the O3 exposures utilized by the NCLAN program have been described as
 4     producing artificial regimes that do not mimic actual conditions.  Lefohn and Foley (1992)
 5     have compared the O3 exposures for the charcoal-filtered (CF) treatments from 13 NCLAN
 6     data sets with clean monitoring sites in the United States. The authors concluded that the
 7     exposures in the CF treatments were lower than those experienced under ambient conditions
 8     at clean O3 monitoring sites and that the CF treatments did not mimic those exposures that
 9     occurred under ambient conditions at the cleanest sites in the United States. Most of these
10     clean monitoring sites, as described  by Lefohn and Foley (1992), are not representative of
11     the crop-growing regions of interest, yet, it is doubtful that the ambient conditions inside the
12     CF chambers would be experienced at any sites in the United States.  The  application of
13     treatment  levels  so low that they are almost never observed anywhere may result  in
14     statistically significant differences that occur when growth comparisons are made  between
15     plants grown in  CF and nonfiltered  (NF) treatments that are not relevant.  Ideally, each
16     exposure in the design should be representative of ambient conditions experienced in the
17     geographic area  of interest and the lowest treatment level (i.e., CF) should be set at the
18     cleanest of these sites.   Because treatment levels are derived from ambient conditions
19     experienced at the research site, CF chambers  may not be identical to ambient conditions at
20     the cleanest site  in the region of interest, but may represent ambient conditions observed
21     somewhere in the world.
22           In addition to  the CF concentration regimes, Lefohn et al.  (1988a) have reported that
23     the highest treatments have a tendency to display bimodal distributions that are unrealistic
24     (Figure 5-9).  At this time, there is  no evidence to suggest whether or not  these higher
25     ambient exposures provide realistic  information on the impact of C^ on plant response.
26           Studies that utilize exposures with peak concentrations above 0.40 ppm may not provide
27     realistic evidence of O3 impact on plant response in the United States. These studies provide
28     limited  evidence for substantiating the value of peak concentrations in influencing response.
29     Consequently, these studies are not  included in this section.
30
       December 1993                          5-117      DRAFT-DO NOT QUOTE OR CITE

-------

oo
3
tn
ve
        ^ 5s £
        &3 w T3

        B il 8
        as
        a
             £1
     §
             s a
             »ff
        rf „
        FB.
     B'
        00
P?l
oo ^ g
          S3

          ll

          I

          i
          - 63
                            Number of Occurrences

                               200     400     600
                                                  Number of Occurrences
                                          800
       50
                      250-
                      300^
                                                                    50
                                                                    j_
                                                        250-
                                                        300-
100

_i_
                                                                            150
Number of Occurrences


      50        100
                                                                          50
00

X
>
3
a-
0'
2
O
N
0
3
CD

100-

-
-
-
150-
-
-

-
200-

                                                                                         250-
                                                                                         300-
                                                                                                          d>
                                                                                                              150
                                                                                                       ^

                                                                                                       X

                                                                                                       >


                                                                                                       g;

                                                                                                       
-------
 1     5.5.2.2  Studies with Two or More Different Patterns of Exposure
 2          Experiments that focus on the structure of exposure have shown that plant response is
 3     differential to temporal patterns of O3 exposure. For crop species, there is evidence to
 4     suggest that plant response is influenced more by higher concentrations than lower
 5     concentrations or exposure duration. Greater response to concentration occurred when plants
 6     were predisposed to low concentrations for a few days or when peaks occurred just prior to
 7     or at maximum leaf expansion  (U.S. Environmental Protection Agency, 1978, 1986).  Plants
 8     exposed to two (or more) different exposure patterns of equal exposure (i.e., same SUMOO
 9     value)  showed greater foliar injury response to:
10
11            1.  The short-term, high-concentration exposure than the longer-term exposure
12               with lower peak concentrations (Heck et al., 1966; Heck and Tingey,
13                1971; Bennett, 1979; Nouchi and Aoki, 1979; Amiro et al., 1984;
14               Ashmore, 1984; Tonneijck,  1984); and
15
16            2.  The exposure that predisposes plants to  low O3 concentrations for a few
17               days prior to a high O3 concentration than exposures  that have a set diurnal
18               pattern of O3 concentrations or less than two days of respite time between
19               high concentrations  (Heck and Dunning, 1967; Johnston and Heagle, 1982;
20               Heagle and Heck, 1974; Runeckles and Rosen, 1977; Mukammal, 1965;
21               Stan and Shicker, 1982).
22
23
24          The studies that applied the same exposure using different patterns of exposure have
25     been reviewed in previous criteria documents (U.S. Environmental Protection Agency, 1978,
26     1986,  1992) and substantiate the role of concentration, temporal dynamics, respite time, and
27     predisposition in influencing the magnitude of plant response to  O3.
28          Musselman et al.  (1983) and Hogsett et al. (1985) were among the first to demonstrate
29     that variable concentrations produced greater effect on plant growth than fixed or set diurnal
30     patterns of exposure of equal total exposure with lower peak concentrations (Table 5-11).
31     Musselman et al. (1986), in  a subsequent experiment,  exposed kidney bean plants to either a
32     simulated ambient or a uniform concentration of equal total exposure and equal peaks (at two
33     levels of 0.30 and 0.40 ppm) and found the effects of the two distributions were not
34     significantly different (Table 5-11).  Consequently, when peak concentrations and total
35     exposures are equal, the diurnal distribution of concentrations appears not to be an important
36     factor (U.S. Environmental Protection  Agency, 1992).
       December  1993                          5419      DRAFT-DO NOT QUOTE OR CITE

-------
t—'
rO
O
                         TABLE 5-11.  A SUMMARY OF STUDIES REPORTING THE EFFECTS OF OZONE
                                  FOR TWO OR MORE EXPOSURE PATTERNS ON THE GROWTH,
                                                PRODUCTIVITY, OR YBELD OF PLANTS
Species
Glycine max L.
Merrill cv. Davis,
Forrest, Bragg, and
Ransom
Medicago saliva L.
Facility'
OTC in
pots
OTC in
pots
Total
Number
Chambers Exposure Patterns
24 16 combinations of CF or
NF over 4 quarters
(31 -days/quarter)
8 Episodic (E), Daily Peak
(DP)
Exposure Concentration (ppm)/Exposure
Duration (ppm-h)
124 days M7 (ppm): CF range from
.016 to .038 over the 4 quarters,
NF range from 0.96 to 0.98 over
the 4 quarters
133 days Equal SUM07 (ppm-h):
DPH=113, DPL=63, EH=117,
EL=72
Equal SUMOO (ppm-h):
DPH=183, DPL=140, EH=193,
Variable Effect Reference
Total Forrest: greater effect in Q3 than Heagle et al.
seed in other quarters. Davis: no (1991)
weight consistent effect Ql, significant
but similar effects for Q2, Q3, and
Q4. Ransom: no significant 03
effects in Ql or Q2, and equal
responses in Ql, Q3, and Q4.
shoot 91 and 67% reductions for EH andHogsett et al.
dry wt DPH (*). Significant difference (1985a)
between E and DP regimes.
Treatment means are ordered
CF
-------
               TABLE 5-11 (cont'd).  A SUMMARY OF STUDIES REPORTING THE EFFECTS  OF OZONE
                            FOR TWO OR MORE EXPOSURE PATTERNS ON THE GROWTH,
3
sr
£2 Species
Phaseolus vulgaris L.
cv. Calif. Dark Red
Kidney Bean
Pinus ponderosa Laws,
PRODUCTIVITY, OR YBELD OF PLANTS
Facility
GC in
pots
OTCin
Total
Number
Chambers
10
15
Exposure Patterns
Initial exposure of .3 ppm
for 3-h and second exp of
.3 ppm at 2-6 (or 1-5)
days after initial exp.
Episodic (E), High Elev
Exposure
Duration
2-6 days
in 1984
and
1-5 days
in 1985
111 days
Concentration (ppm)/Exposure
(ppm-h)
Equal maximum concentration of
0.30 ppm.
Equal SUMOO (ppm-h):
Variable
total dry
weight
leaf
Effect6
Reductions due to the second
exposure were significant when
exposures were 3-6 days apart in
1984 and 5 days apart in 1985.
At low level, 64 and 0%
Reference
McCool et al. (1988)
Hogsett and Tingey (1990)
Populus tremuloides   pots
michx.
                                (HE), Daily Peak (DP)
DPH=HEH=EH=170,
HEL=EL=122.
 stem,  reductions for E and HE(*).  At
 stem,  high level, 42 %, 75 %, and 7 %
root, dry reductions for E, HE, and DP(*).
 weight  Treatment means are ordered
       E
-------
 1          One recent study exposed bean plants to two consecutive exposures of 0.30 ppm for
 2     3 h per day in the rapid vegetative growth stage and showed greater reductions in total dry
 3     weight when exposures were three to six days apart (McCool et al., 1988) (Table 5-11),
 4     consistent with earlier results on the role of predisposition in influencing response (e.g.,
 5     Hogsett et al., 1988). Predisposition to a high concentration above the level that causes
 6     visible injury may increase plant sensitivity  over tune (Mukammal, 1965).  As a result, the
 7     subsequent response to a high concentration following recovery may be greater than
 8     experienced in prior exposures. In future modeling efforts, this phenomenon may have to be
 9     taken into consideration by the weighting of hourly concentrations for properly characterizing
10     plant exposure.
11           Sensitivity of plants to O3 is a function of stomatal conductance and varies with
12     phenology.  To test the role of phenology, Heagle et al. (1991) applied 16 patterns of
13     exposure in combinations of either charcoal-filtered (CF) or nonfiltered (NF) for each quarter
14     of the experimental period (31 days/quarter) (Table 5-11).   The authors concluded that plant
15     response was  differential to phonological stage of development and that exposures during
16     mid- to late-growth stages caused a greater yield loss than early exposures.  For crops,
17     foliage appears to be most sensitive to O3 just prior to or during maximum leaf expansion
18     (U.S. Environmental Protection Agency, 1978). These results are consistent with earlier
19     studies (Lee et al., 1987) that  reported better statistical fits to response using exposure
20     indices that preferentially weighted hourly O3 concentrations during the period of anthesis to
21     seed fill.
22           There is very limited information on the nature of seedling response to O3 (see
23     Section  5.3.7) and much less is known about the  role of exposure-dynamic factors (e.g.,
24     concentration, duration, respite time, temporal variation) in influencing biomass response in
25     long-lived species.  In a study by Hogsett and Tingey (1990), ponderosa pine and aspen
26      seedlings were exposed to three different exposure patterns of equal SUMOO over a  5-mo
27      growing season (Table 5-11).   One pattern simulated ambient conditions at high-elevation
28      sites remote from urban influence.  A second pattern (i.e., episodic) was representative of
 29      ambient conditions at low-elevation sites at rural  or near-urban locations.  A third pattern
 30      was artificial and had a diurnal pattern rising to a peak at 2 ppm, repeated daily  for the
 31      length of the experimental period.  Growth reductions  in both ponderosa pine and aspen were

        December 1993                          5-122      DRAFT-DO NOT QUOTE OR CITE

-------
 1     greatest in the episodic exposure pattern, which had the largest peak concentrations of the
 2     three patterns.  The smallest growth reductions in both species were observed with the high-
 3     elevation pattern that had peak concentrations less than 0.10 ppm.  The authors concluded
 4     that temporal pattern and concentration were important in influencing long-term growth
 5     response of tree seedlings, just as in crops, and, consequently, should be considered in
 6     measures of exposure.
 7          When yield is considered, a number of exposure-dynamic factors, including
 8     concentration, temporal pattern, predisposition and respite times, as well as phenological
 9     stage of plant development, have been shown to influence the impact of O3 on plant
10     response.  Evidence from studies of kidney bean (Musselman et al., 1983), alfalfa (Hogsett
11     et al.,  1985a), tobacco (Heagle et al.,  1987), soybean (Heagle et al., 1986), ponderosa pine
12     and aspen (Hogsett and Tingey, 1990) suggests that concentration and temporal variation of
13     exposure are important factors hi influencing biomass production and, consequently become
14     considerations in measures of exposure.  Because the SUMOO index weights all
15     concentrations equally, the SUMOO is inadequate for characterizing plant exposure to
16     O3 (Lefohn et al.,  1989).  Other factors, including predisposition time (McCool et al., 1988)
17     and crop development stage (Heagle et al., 1991), contribute to variations  in biological
18     response, which suggests the need for weighting O3 concentrations to account for
19     predisposition time and phenology.  However, the roles of predisposition and phenology in
20     influencing plant response vary with species and environmental conditions  and are not
21     understood well enough to allow specification of a weighting function for use in
22     characterizing plant exposure.
23
24     5.5.2.3  Combinations of Years, Sites, or Species:  Comparisons of Yield Losses with
25              Different Exposure Durations
26          Duration has not been a focus in experimental designs of studies that applied two or
27     more exposure regimes over the growing season. Several lines of evidence suggest that the
28     ultimate yield depends upon the cumulative impact of repeated peak concentrations (U.S.
29     Environmental Protection Agency, 1986,  1992) and that O3-induced reductions in growth are
30     linked  to reduced photosynthesis, which is impaired by the cumulative O^  exposure (Reich
31     and Amundsen, 1985; Reich, 1987;  Pye,  1988). In the Agency's reviews  of the literature
32     (U.S. Environmental Protection Agency, 1986, 1992), EPA concluded that, "When plant
       December 1993                          5_123       DRAFT-DO NOT QUOTE OR CITE

-------
 1      yield is considered, the ultimate impact of an air pollutant on yield depends on the integrated
 2      impact of the pollutant exposures during the growth of the plant."  As a measure of plant
 3      exposure, the appropriate index should differentiate between exposures of the same
 4      concentration but of different duration. For example, a mean index calculated over an
 5      unspecified time cannot accomplish this (Lefohn et al., 1988a; Hogsett et al., 1988; Tingey
 6      et al., 1989, 1991; U.S. Environmental Protection Agency, 1986, 1992).
 7           The paper by Lefohn et al. (1988a), reviewed previously in U.S. EPA (1992) along
 8      with published criticisms and responses, was the first to fit a common response model to
 9      combined data from two replicate studies of unequal duration (71 and 36 days for the 1982
10      and 1983 wheat studies, respectively,  conducted at Ithaca, NY) to specifically test the
11      importance of duration in influencing plant response.  Greater yield losses occurred in 1982
12      which can partially be attributed to the longer duration. Because the mean index ignores the
13      length of the exposure period, the  year-to-year variation in plant response was minimized by
14     the use of several cumulative indices rather than the mean.  Lefohn (1988) and Lefohn et al.
15      (1988b) concluded that duration has value in explaining variation in plant response and that a
16     cumulative-type index was preferred over a mean or peak index based on statistical fit.
17          When O3 effects are the primary cause of variation in plant response, plants from
18     replicate studies of varying duration showed greater reductions in yield or growth when
19     exposed for the longer duration (Lee et al., 1991; Olszyk et al., 1993; Adaros et al., 1991a)
20     (Table 5-12 Part A).  Using NCLAN data for wheat, cotton, kidney bean, and potato (from
21     Penn State) from  replicate studies  with markedly different exposure durations, Lee et al.
22     (1991) showed that year-to-year variations in the magnitude of relative yield loss were
23     minimized by the use of exposure indices that are cumulative and weight peak concentrations
24     more than low concentrations, indicating that O3 effects are cumulative (Figure 5-10).
25     Olszyk et al. (1993), using the two NCLAN cotton studies summarized by Temple et al.
26     (1985) and Lee et al.  (1991), in addition to cotton studies replicated at four sites in
27     California's San Joaquin Valley over two years, tested and compared various exposure
28     indices (SIGMOID, SUM06,  M7, and 2ndHDM) based on statistical fit of a common
29      response model.  A Weibull response model with variance components was fit to the
30      combined data and used to test for a  common response (Gumpertz and Rawlings, 1991,
31      1992; Gumpertz and Pantula, 1992).  The likelihood ratio test of parallel exposure-response

        December 1993                          5-124     DRAFT-DO NOT QUOTE OR CITE

-------
              TABLE 5-12.  A SUMMARY OF STUDIES REPORTING THE EFFECTS OF OZONE ON THE GROWTH,
                  PRODUCTIVITY, OR YIELD OF PLANTS FOR TWO OR MORE REPLICATE STUDIES HAVING
                     EQUAL TOTAL EXPOSURES AND EITHER VARYING DURATIONS (PART A) OR SIMILAR
                                                              DURATIONS (PART B)
Part A
Species
Brassica napus L.
var. napus
cv. callypso
Gossypium
Hirsutum L.
cv. Acala SJ2

T- •!• 3
Facility
OTC in
pots

OTC



Total No.
of Plots
'87: 18
'88: 24
'89: 16
'81: 12
'82: 12



'87:
'88:
'89:
'81:
'82:


Duration
05-13 to 08-10 (89)
05-02 to 08-24 (113)
05-08 to 08-01 (84)
07-06 to 09-15 (72)
06-04 to 09-09 (98)



'8V:
'88:
'89:
'81:
138
'82:
111
Concentration (ppm)/ Exposure (ppm-h)
M24 (MS) in ppb range from 5 (9) to 16 (43).
M24 (M8) in ppb range from 3 (5) to 16 (48).
M24 (M8) in ppb range from 6 (5) to 22 (62).
M7 (SUM06) range from 18 ppb (0 ppm-h) to
(68).
M7 (SUM06) range from 12 ppb (0 ppm-h) to
(71).
Variable
seed
dry
weight
lint
dry wt

'87: 27%
'88: 18%
'89: 11%
45% and
57% and
Effect0
reduction at M8=43 ppb
reduction at M8 = 48 ppb
reduction at MS = 62 ppb

(***).
(***).
(***).
66 % reductions at M7= 1 1 1 ppb .
60 % reductions at

SUM06=68 ppm-h.




Reference
Adaros et al.
(1991c)

Lee et al.
(1991),
Olszyk et al.
(1993)
      Hordeum vulgare
      L.
      cf. Arena and
      Alexis

      Phaseoulus
      vulgaris L.
      cv. Calif Dark
      Red
      Kidney Bean
OTC in    '88: 24   '88: 04-29 to 08-15 (108)
pots      '89: 16   '89: 05-08 to 08-15 (99)
OTC      '80: 20   '80: 08-20 to 09-10 (22)
         '82: 20   '82: 08-11 to 10-06 (57)
 '88: M8 (max 8-h mean) in ppb range from 5 (15) to seed
 48 (89).                                 dry wt
 '89: M8 (max 8-h mean) in ppb range from 11 (27)
 to 62 (101).
'80: M7 (SUM06) range from 24 ppb (0 ppm-h) to
139 (19).
'82: M7 (SUM06) range from 19 ppb (0 ppm-h) to
110(40).
seed
dry wt
Arena: 14% (*) and 6% (NS) reductions at Adaros et al.
M8=48ppb.                      (1991b)
Alexis: No reductions at M8=48 ppb
(NS).

13% and 59% reductions at M7= 110 ppb. Lee et al.
28% and 8% reductions at            (1991)
SUM06= 19 ppm-h.
 C,   Phaseolus vulgaris OTC in
 Trt   L.            pots
 H   cf. Rintintin
 O
 o
 1^   Solanum        OTC
 O   Tuberosum L.
 "   cv. Norchip
O
 S   Triticum aestivum OTC
 ,j   L., cv. Vona
         '881:4   '88 I: 06-15 to 08-04 (51)  I. M8 (Max) in ppb range from 3 (19) to 48 (70).
         '88 H: 6  '88 H: 07-24 to 08-29 (37)  n. M8 (Max) in ppb range from 2 (19) to 50 (105).
         '89 HI: 8  '89 ffl: 06-04 to 07-25 (52) ffi. M8 (Max) in ppb range from 6 (26) to 109
                                     (159).
         '85: 15   '85: 06-14 to 08-22 (70)
         '86: 39   '86: 06-20 to 08-20 (62)
         '82: 20   '82:05-18 to 07-17 (61)
         '83: 12   '83: 06-12 to 07-17 (36)
'85: M7 (SUM06) range from 22 ppb (0 ppm-h) to
85 (47).
'86: M7 (SUM06) range from 24 ppb (0 ppm-h) to
88 (38).
'82: M7 (SUM08) range from 21 ppb (0 ppm-h) to
95 (40).
'83: M7 (SUM08) range from 26 ppb (0 ppm-h) to
96(21).
pod    I. 2% reduction at M8=48 ppb (NS).    Bender et al.
dry    H. 0% reduction at M8=50 ppb (NS).   (1990)
weight  m. 0% (NS) and 47% (*) reductions at
       M8=50 and 109 ppb.

tuber   42% and 25% reductions at M7 = 85 ppb.  Lee et al.
weight  32% and 27% reductions at 12-H        (1991)
       SUM06=38 ppm-h.

seed    74% and 49% reductions at M7=95 ppb.  Lefohn et al.
dry wt  49% and 62% reductions at           (1988),
       SUM08=21 ppm-h.                 Lee et al.
       55% and 60% reductions at 7-h         (1991)
       SUM06=22 ppm-h.

-------
 I
 u>
                TABLE 5-12 (cont'd).  A SUMMARY OF STUDIES REPORTING THE EFFECTS OF OZONE ON THE
                 GROWTH, PRODUCTIVITY, OR YIELD OF PLANTS FOR TWO OR MORE REPLICATE STUDIES
                       HAVING EQUAL TOTAL EXPOSURES AND EITHER VARYING DURATIONS  (PART A)
                                                       OR SIMILAR DURATIONS (PART B)
     Part A
     Species
Facility
                              Total No.
                               of Plots
                                             Duration
Concentration (ppm)/ Exposure (ppm-h)
                                                                              Variable
                                                                                                  Effect"
                                                                                                                       Reference
     Triticum aestivum OTC in    '88: 6
     L., cv. Star and   pots       '89: 10
     Turbo
                                      '88: 04-27 to 08-23 (118)
                                      '89: 05-09 to 08-15 (98)
                                     '88: M8 (Max,SUM06) in ppb range from 4 (58,0)  seed
                                     to 51 (106,8.2).                            dry wt
                                     '89: M8 (Max,SUM06) in ppb range from 10 (34,0)
                                     to 113 (162,87).
                                           Star: 20% (*) and 9% (NS) reductions at   Adaros et al.
                                           M8 = 51 ppb.                        (1991a)
                                           Turbo: 25% (*) and 31% (*) reductions at
                                           M8 = 51 ppb.
     Triticum aestivum OTC in
     L., cv. Star and   pots
     Turbo
                             '88:24   '88: 04-29 to 08-15 (108)   '88: M8 (max 8-h mean) in ppb range from 5 (15) to seed    Star: 26% (*) and 12% (*) reductions at   Adaros et al.
                             '89:16   '89:05-08 to 08-15 (99)    48(89)                                   dry wt   M8 = 48ppb.                       (1991b)
                                                           '89: M8 (max 8-h mean) in ppb range from 11 (27)          Turbo: 34% (*) and 17% (*) reductions at
                                                           to 62 (101)                                       M8 = 48ppb.
Ul
t—*
N)
     PartB.
     Glycine max L.
     Merr.
     cv. Davis
     Qlycine max L.
     Merr.
     cv. Williams
                    OTC in
                    pots
                    OTC
        '77:8    '77: 06-17 to 10-10(116)  '77: M7 (max) in ppb range from 27 (78) to 154
        '78: 8    '78: 06-28 to 10-21 (116)  (277).
                                     '78: M7 (max) in ppb range from 28 (84) to 131
                                     (241).
                             '81: 31    '81: 07-20 to 09-22 (65)
                             '82: 31    '82: 07-14 to 09-22 (71)
                             '83: 31    '83: 07-23 to 09-23 (63)
                                     '81: M7 in ppb range from 15 to 64.
                                     '82: M7 in ppb range from 17 to 99.
                                     '83: M7 in ppb range from 19 to 132.
                                   seed     47% and 37% reductions at M7=131 ppb. Cure et al.
                                   dry wt                                   (1986),
                                                                           Heagle et al.
                                                                           (1983)

                                   bean     28%, 20%, and 32% reductions at       Heggestad
                                   dry     M7=64ppb.                       and
                                   weight   43 % and 41 % reductions at M7=99 ppb  Lesser
                                           in '82 and '83                      (1990),
                                                                           Heggestad
                                                                           et al. (1988)
O   Medicago saliva   OTC
O   L. cv. WL-514
25
O   pjnus rigida      OTC in
H   Mill.            pots
                              '84:30   '84: 03-16 to 10-10 (209)   '84: M12 in ppb range from 16 to 109.
                              '85:30   '85: 03-23 to 10-09 (201)   '85: M12 in ppb range from 10 to 94.
                             Exp. 1: 4  Exp. 1: 13 weeks
                             Exp. 2: 4  Exp. 2: 13 weeks
                                     1: M8 in ppb range from 0 to 200 ppb (U).
                                     2: M8 in ppb range from 0 to 200 ppb (U).
                                   top     29% (*) and 25% (*) reductions at       Temple et al.
                                   drywt  M12=94ppb.                      (1988)

                                   total    49% and 46% reductions at M8=200 ppb. Schier et al.
                                   dry wt                                   (1990)

-------
 §
TABLE 5-12 (cont'd). A SUMMARY OF STUDDZS REPORTING THE EFFECTS  OF OZONE ON THE
 GROWTH, PRODUCTIVITY, OR YIELD OF PLANTS FOR TWO OR MORE REPLICATE STUDIES
       HAVING EQUAL TOTAL EXPOSURES AND EITHER VARYING DURATIONS (PART  A)
                                     OR SIMILAR DURATIONS (PART B)
PartB
Species
Pinus taeda L.
Total No.
Facility of Plots Duration
GC in '86: 15 '86: 09-15 to 12-04 (81)
pots '87: 15 '87: 07-27 to 10-15 (81)
Concentration (ppm)/ Exposure (ppm-h)
'86: SUMOO in ppm-h range from 0 to 99 (U).
'87: SUMOO in ppm-h range from 0 to 99 (U).
Variable Effect6
total 43 % and 28 % reductions at
dry wt SUMOO = 99 ppm-h
Reference
Shafer et al.
(1993)
      Picea rubens     OTC in    '87: 12
      Sarg.           pots      '88: 12
£j    Pisum sativum L.  ZAPS     '86: 14
      cv. Puget                 '87: 14
 O   Populus         OTC in    '88: 18
 I*   tremuloides      pots      '89: 18
 (L:   Michx clones
                     '87: 05-30 to 12-15 (199)  '87: SUMOO in ppm-h are 32, 61, 91 and 119.
                     '88: 06-01 to 12-01 (184)  '87: SUMOO in ppm-h are 36, 70, 101 and 135.
                     '86: last 58 days         M12 and D25 (# days with 1-h cone >25 ppb)
                     '86: last 52 days         used in simple linear regression
                    '88: 07-19 to 09-27 (71)   '88: SUMOO in ppm-h are 5.0, 10.0, and 19.4 (U).
                    '89: 07-20 to 09-20 (64)   '89: SUMOO in ppm-h are 7.7, 15.4, and 26.4 (U).
total
dry wt
averaged across all families.
Individual families show similar
reductions, e.g., 35% and 33% reductions
at SUMOO = 99 ppm-h for family 5.56,
14% and 12% reductions at
SUMOO=99 ppm-h for family 1.68.

0% (NS) reduction in biomass after 1st yr,  Alscher et al.
8% (*) reduction at SUMOO= 135 ppm-h   (1989)
after 2nd year of exposure             Amundsen
                                etal.
                                (1991)
pea    0 % reductions at M12 =100 ppb
fresh wt based on linear regression models
stem and 36% (*) and 40% (*) reductions at
leaf dry SUMOO= 19.4 ppm-h.
wts
                                Runeckles
                                etal.
                                (1990)

                                Karnosky
                                etal.
                                (1992)
 tj   Triticum aestivum  OTC
 O   L-. cv. Albis
O
CH   Triticum aestivum  OTC
Q   L., cv. Albis
            '86: 12   '86: 05-06 to 07-31 (86)    '86: M24 (max) in ppb range from 12 (61) to 47
            '87:16   '87: 04-27 to 08-10 (92)    (181).
            '88: 16   '88: 05-04 to 08-01 (89)    '87: M24 (max) in ppb range from 12 (54) to 45
                                         (175).
                                         '88: M24 (max) in ppb range from 17 (65) to 45
                                         (148).
            '89: 24   '89: 05-16 to 08-14 (91)    '89: M7 (SUM06) range from 18 ppb (0 ppm-h) to
            '90: 24   '90: 05-14 to 08-09 (88)    62 (3.8).
                                         '90: M7 (SUM06) range from 17 ppb (0 ppm-h) to
                                         71 (5.6).
seed    '86: 61% reduction at M24=47 ppb.     Fuhrer etal.
dry wt  '87: 27% reduction at M24=45 ppb.     (1989)
       '88: 65% reduction at M24=45 ppb.
seed    29 % and 22 % reduction at M7=62 ppb.   Fuhrer et al.
dry wt  29% and 17% reduction at             (1992)
       SUM06=3.8 ppm-h.

-------
V
oo
            TABLE 5-12 (cont'd). A SUMMARY OF STUDIES REPORTING THE EFFECTS OF OZONE ON THE
            GROWTH, PRODUCTIVITY, OR YIELD OF PLANTS FOR TWO OR MORE REPLICATE STUDffiS
                 HAVING EQUAL TOTAL EXPOSURES AND EITHER VARYING DURATIONS (PART A)
                                        OR SIMILAR DURATIONS (PART B)
Part B Total No.
Species Facility8 of Plots Duration
Triticum aestivum OTC
L., cv. Severn,
Potomac, Oasis,
MD55 18308
'84: 20 '84: 05-14 to 06-22 (40)
'85: 20 '85: 05-06 to 06-15 (41)
Concentration (ppm)/ Exposure (ppm-h) Variable Effect
'84: M4 (AOT03) in ppb (ppb-h) range from 32 (0) seed
to 93 (10). dry wt
'85: M4 (AOT03) in ppb (ppb-h) range from 30 (0)
to 86 (9).
31 % (*) and 956 (NS) reductions at
M4 = 86ppb.
Reference
Slaughter
et al.
(1989)
    *GC = controlled environmental growth chamber or CSTR, OTC= open-top chamber, ZAPS=zonal air pollution system.
    bU = Uniform.
    c* = significant at the 0.05 level, NS= not significant.

-------
        1.00ft
                      Cotton
                 Wheat
                   .08   .12    i  20 40  60
               M-7 (ppm)    Sum06 (ppm-h)

                    Kidney Bean
         0.03 0.06
         M-7 (ppm)   Sum06 (ppm-h)

                 Potato
                                 20    40
              M-7 (ppm)    Sum06 (ppm-h)
          0.03  0.06  0.09 0 20    40
          M-7 (ppm)    Sum06 (ppm-h)
Figure 5-10. Comparison of the Weibull exposure-response functions and its predicted
            relative yield loss (PRYL) curves (relative to 0 ozone) using M-7 and
            daytime SUM06 for replicate years of National Crop Loss Assessment
            Network Program's data for (A) and (B) cotton (var. Acala SJ-2), (C) and
            (D) wheat (var. Vona), (E) and (F) kidney bean (var. California light red),
            and (G) and (H) potato (var. Norchip), respectively.  Mean dry weights
            and the Weibull exposure-response functions for replicate studies are given
            in the top portion of the graphs (Lee et al.,  1991).
December 1993
5-129
DRAFT-DO NOT QUOTE OR CITE

-------
 1     curves was statistically significant for M7 and 2ndHDM for at least one set of cotton data,
 2     indicating significant differences in the magnitude of response across years and/or sites.
 3     On the other hand, the SIGMOID and SUM06 indices resulted in consistent patterns of
 4     response for both sets of cotton data, as well as between sets of cotton data (Figure 5-11).
 5     The authors concluded that the peak-weighted, cumulative indices minimized the temporal
 6     and spatial variations in crop yield and better predicted cotton yield responses than the M7 or
 7     2ndHDM indices.  The mean and peak indices did not differentiate between exposure seasons
 8     of differing duration and could not account for year-to-year differences in response.
 9          The results of European studies with wheat (Adaros et al., 1991a,b), spring rape
10     (Adaros et al.,  1991c), barley (Adaros et al., 1991b) and kidney beans (Bender et al.,  1990),
11     using data from replicate studies with varying duration, are less conclusive as to the role of
12     duration in determining plant response (Table 5-12 Part A).  Exposures are reported using a
13     mean index. Adaros et al. (1991a) showed a greater reduction in above ground dry weight
14     when exposed for the longer duration for wheat cultivar,  Star, but not for cultivar,  Turbo
15     (Figure 5-12).  Adaros et al. (1991b), in another two-year study with barley (cv. Arena and
16     Alexis) and wheat (cv. Star and Turbo)  involving mixtures of O3, SO2, and NO2, showed
17     greater reductions in yield when exposed for the longer duration for all species and cultivars
18     except barley cv. Alexis (Table 5-12 Part A).  Ozone effects were insignificant in both years
19     for barley cv. Alexis.  The authors did not attribute the differential response in growth and
20     yield to any single factor but the data suggested that 03 effects are cumulative.  When
21     O3 exposure is the primary source of response, the mean exposure index of unspecified
22     duration could not account for the year-to-year variation in response.
23           The role of duration  in influencing growth or yield is unclear for the other studies
24     because of the following limitations in the data:
25
26             1. Treatment levels were below the levels to induce injury or damage to
27                kidney bean plants in two of the three years.  None of the years produced a
28                significant O3 effect at or below 70 ppb concentration (Bender et al.,
29                1990). Similarly, the study with barley  showed no significant O3 effects.
30
31             2. Differences in growing conditions and varying kinds of interactions
32                between O3, SO2, and NO2 resulted in different sizes of control plants of
33                spring rape over years  and affected the magnitude of response to O3.

        December 1993                           5-130      DRAFT-DO NOT QUOTE OR CITE

-------

3
en
                 Predicted Relative Yield Loss (%)
Predicted Relative Yield Loss (%)

-------
       120
        90 -
f 60
        30
             Star
             Total Biomass
            	 1988
            	1989
             Grain Yield
            	1988
                                I
                                        Turbo
                                         XV
                                                  I
                    0.015      0.03        0          0.015
                               Ozone Concentration (ppm)
                                                            0.03
                        0.045
Figure 5-12.  Relative effect of ozone on growth and yield of spring wheat cultivars (var.
             Star and Turbo) from two growing seasons (Adaros et al., 1991a).
       Compared to 1987, yield of control plants increased by 32% in 1988 and by
       94% in 1989 (Adaros et al., 1991c).  Consequently, the evidence of duration
       as the primary cause of differences in response over years was difficult to
       substantiate.
     When durations were nearly equal, plant response to O3 were similar for 2- or 3-year
studies with alfalfa (Temple et al., 1988), pea (Runeckles et al., 1990), soybean (Heagle
et al., 1983; Heggestad and Lesser, 1990; Cure et al., 1986), wheat (Fuhrer et al., 1989,
1992), aspen clones (Karnosky et al., 1992), loblolly pine (Shafer et al., 1993), and pitch
pine (Schier et al., 1990) (Table 5-12 Part B). For example, year-to-year variations in wheat
yield response to O3 were small for the three years having durations between 86 and 92 days
to allow pooling of the data to fit a common Weibull model using Rawling's solar-radiation
December 1993
                                    5-132
DRAFT-DO NOT QUOTE OR CITE

-------
weighted mean index (Fuhrer et al., 1989) (Figure 5-13).  Different growing conditions were
reported in a number of studies (Shafer et al., 1993; Fuhrer et al.,  1989) but found no
interaction between O3 and climatic effects.  On the other hand, Slaughter et al. (1989)
reported reductions in wheat grain yield of 69% and 9% in a two-year study having equal
durations, which the authors attribute to differences in rainfall  and temperature.
Environmental conditions in 1985 favored greater photosynthate partitioning for grain
development rather than for vegetative growth, resulting in larger plants in 1985.   Air
pollution effects may not have been the primary source of variation in response and,
consequently, the data are unable to substantiate the role of duration in influencing response.
\.
w3^ X-NX-
"X^\
S--P

00 0.02 0.04 0.06 0.08
Year
& - 1986
— -B— 1987
......4..... 1988
— e — Combined


^^~^
i
0.10 0.1
                         Mean Weighted Ozone Concentration (ppm)
 Figure 5-13. Weibull exposure-response curves for the relative effect of ozone on grain
             yield of spring wheat for three years, individually and combined (Fuhrer
             et al., 1989).
 December 1993
5-133      DRAFT-DO NOT QUOTE OR CITE

-------
 1          These studies report plant response as a function of a mean exposure index and do not
 2     evaluate or compare various exposure indices based on statistical fit.  In a series of three
 3     papers that examined the response of spring wheat to O3 at higher elevations, Grimm and
 4     Fuhrer (1992a,b) and Fuhrer et al. (1992) conducted a 2-year study in which the flux of
 5     O3 was determined in open-top chambers.  Plants were exposed to O3 for periods  lasting
 6     44 and 50 days in 1989  and 1990, respectively and flux measurements were taken repeatedly
 7     over the experimental period. In addition to O3 flux, exposures were characterized using
 8     M7, M24,  SUM06, and the solar  radiation-weighted mean index (Rawlings et al., 1988).
 9     The quadratic response curves relating the various indices with grain yield showed
10     year-to-year variations were minimized using the mean O3 flux index (Figure 5-14).  The
11     other three exposure indices showed slightly greater yield losses in 1989 than in 1990, in
12     contrast with longer exposure in 1990 and drier conditions in 1989.  The authors concluded
13     that the O3 flux related well with  yield because the mean flux incorporated environmental
14     factors, canopy structure, and physiological processes, which affected the uptake of O3 from
15     the air to the leaf interior.  The measures of ambient condition ignored these factors and
16     consequently, were unable  to account for all of the year-to-year variability hi wheat response.
17     The authors suggested that  O3 flux was a surrogate of Fowler and Cape's (1982) "pollutant
18     absorbed dose" and appeared to be the relevant measure for use hi relating exposure and
19     plant response.
20           Alscher et al.  (1989)  and Amundson et al. (1991) report on the impact of Oj on
21     growth,  injury, and biomass response of 2-year-old red spruce seedlings  after 1 and 2 years
22     of exposure, respectively.  Exposures were characterized  using the M12  (or M7), M24, and
23     SUMOO indices.  No  significant O3 effects on biomass were detected hi 1987 (Alscher et al.,
24      1989) because stomatal conductances in red spruce are inherently low and, consequently,
25     result in low rates of pollutant uptake (Seiler  and Cazell,  1990).  However, in the second
26      year, O3 reduced leaf and  root starch, increased foliar antioxidant content, and reduced
27      biomass of 1988 fixed-growth foliage. However, O3 effects on biomass were slight hi the
28      second year.  The authors  concluded O3 effects are cumulative because the  onset of damage
29      occurred in the second year rather than the first year of exposure.
30           When the concentrations are above the levels hi which injury and damage occur, plant
31      response is influenced by exposure duration.  The results of these studies are hi general

        December 1993                          5-134      DRAFT-DO NOT QUOTE OR CITE

-------
               1
           1.2
           1.0
           0.8
           0.6
           0.4
           0.2

            0,
                                               (a)
             0  20  40 60  80  100 120 140 160 180
                     7 h day1 (ng nf)
0  20  40 60  80  100 120 140  160 180
   Radiation weighted mean (ng nf)
                                                     • 1.2
                                                       1.0
                                                       0.8
                                                       0.6
                                                       0.4
                                                       0.2
                                                        0
                                                      20
                                             40   60   80   100  120  140
                                              Sum06 (mg rrt3 h)
                                                              20   40   60   80   100
                                                                Ozone flux (pg nf mlri1)
                                                                               120
       Figure 5-14.  Quadratic exposure-response curves for the relative effect of ozone on
                     grain yield of spring wheat in 1989 and 1990 using four different exposure
                     indices (a-d) (Fuhrer et al., 1992).
 1
 2
 3
 4
 5
 6
 7
 8
 9
10
11
12
13
agreement that O3 effects are cumulative and the ultimate impact of long-term exposures tp
O3 on crops and seedling biomass response depends on the integration of repeated peak
concentrations during the growth of the plant.  Consequently, the mean or peak indices are
inappropriate since the length of exposure is unspecified and these indices cannot differentiate
among exposures of the same concentration but varying in duration.  These results support
the conclusion that an appropriate O3 index should cumulate hourly  concentrations in some
fashion to reflect the nature of O3 on plant response.  Fuhrer et al. (1992) suggested that the
weighting function should reflect the relationship between ambient condition and internal
O3 flux, consistent with the mode of action of 03 on plants and with earlier findings that
peak-weighted, cumulative indices give better predictions of plant response than mean or
peak indices.
       December 1993
                                         5-135
                                       DRAFT-DO NOT QUOTE OR CITE

-------
 1     5.5.2.4  Comparisons of Measures of Exposure Based on Reanalysis of Single-Year,
 2              Single-Species Studies
 3          Studies cited in previous sections focused on the role of the structure of exposure in
 4     influencing plant response but do not specifically identify the weighting function for use in
 5     characterizing plant exposure to O3.  In addition to these types of studies, other studies have
 6     focused on comparison of measures of exposure based on reanalysis of single-year, single
 7     species studies. The variety of statistical approaches used to relate exposure and plant
 8     response range from informal description of the distributions of O3 concentrations  associated
 9     with response to more formal regression-based procedures.
10          The regression approach is designed to select those exposure indices that properly order
11     and space the treatment means along the horizontal axis  to optimize the fit of a linear or
12     curvilinear model.  However, because the experimental designs are not designed to evaluate
13     various indices, the power of the regression approach to identify the important exposure-
14     dynamic factors influencing plant response is less than desirable (Lefohn et al., 1992a).
15     Consequently, these retrospective studies provide less substantiating evidence of the role of
16     exposure-dynamic factors (e.g., concentration, duration, temporal pattern, and respite time)
17     than those  studies with experimental designs and analyses that focus on specific components
18     of exposure.
19          Most of the early retrospective studies reporting regression results using data from the
20     NCLAN program and/or from Corvallis, Oregon (Lee et al., 1987, 1988; Lefohn et al.,
21      1988a: Tingey et al., 1989) or using data collected by Oshima (U.S. Environmental
22     Protection Agency, 1986; Musselman et al., 1988) were in general agreement and
23     consistently favored the use of cumulative peak-weighted exposure indices.  These studies
24     have been  previously reviewed by the Agency (U.S. Environmental Protection Agency,
25      1992). Lee et al. (1987) suggested that exposure indices that included all the data (24 h)
26     performed better than those that used only  7 h of data; this is consistent with the conclusions
27      of Heagle  et al. (1987) that found plants receiving exposures for an additional 5 h/day
28      showed 10% greater yield loss than those exposed for 7-h/day. In a subsequent analysis
29      using  more of the NCLAN data, Lee et al. (1988) found the "best" exposure index was a
30      general phenologically weighted, cumulative-impact index (GPWCI) with sigmoid weighting
31      on concentration and a gamma weighting function as surrogate of time of increased plant
 32      sensitivity to O3.  For most  cases, Lee et al. (1987) computed their exposure indices based
        December 1993                           5-136      DRAFT-DO NOT QUOTE OR CITE

-------
 1     on the daylight exposure periods used by the NCLAN investigators.  The exposure indices
 2     with minimum RSS were those indices that (1) cumulated hourly O3 concentrations over the
 3     growth of the plant, (2) gave preferential weighting to peak concentrations, and
 4     (3) phenologically weighted the exposures to emphasize concentrations during the plant
 5     growth stage. The paper by Tingey et al.  (1989) is a summarization of the results in Lee
 6     et al. (1988) and shows the limitations of the mean index.
 7          Lefohn and Foley (1992) characterized the NCLAN exposures that had a SUM06 level
 8     closest to those that predicted a 20% yield loss,  using the exposure-response  equations as
 9     reported in Lee et al. (1991) and Tingey et al. (1991).  Lefohn and Foley (1992)
10     characterized the hourly average concentrations using percentiles, HRS06, HRS10, SUM06,
11     and W126 for each of 22 NCLAN studies.  The authors noted that the frequent occurrence in
12     many cases  of high hourly concentrations (^:0.10 ppm) may have been partly responsible for
13     the 20% yield loss. The number of hourly average concentrations ranged from 0 to  515 with
14     only one of the 22 NCLAN experiments experiencing no hourly average concentrations
15     ^0.10 ppm, while the remaining experiments experienced multiple occurrences ^0.10 ppm.
16     The repeated occurrences of high hourly average concentrations were a result of the  NCLAN
17     protocol (Table 5-13).  As a result of their analysis, Lefohn and Foley (1992) and Lefohn
18     et al. (1992b) stressed that because the NCLAN experiments contained peak  hourly average
19     concentrations, it is important that any index selected to characterize those regimes
20     responsible  for growth reduction adequately capture the presence of these peak concentrations
21     when attempting to predict biological responses using actual ambient air quality data.
22          For example, Tingey et al. (1991), using mostly NCLAN data, identified 24.4  ppm-h
23     as  the SUM06 value, calculated over a 3-mo period, that would protect 50% of the NCLAN
24     crops analyzed at the 10% yield reduction  level.  There are monitoring sites  in the United
25     States that experience 3-mo cumulative SUM06  values greater than 24.4 ppm-h, but  do not
26     experience frequent occurrences of hourly  average concentrations >  0.10 ppm. For
27     example, 24% (1987), 10% (1988), 30% (1989), 25% (1990), and 31% (1991) of the rural
28     agricultural  sites listed in the U.S. EPA  AIRS database experienced 3-mo cumulative SUM06
29     values greater than 24.4 ppm-h, but experienced fewer than 11 hourly average concentrations
30     equal to or greater than 0.10 ppm.  Lefohn and  Foley (1992) noted that agricultural  crops
31     grown at a site experiencing a 3-mo cumulative  SUM06 value greater than 24.4 ppm-h, but

       December 1993                         5437     DRAFT-DO NOT QUOTE OR CITE

-------
TABLE 5-13. SUMMARY OF OZONE EXPOSURES THAT ARE CLOSEST TO THOSE PREDICTED FOR
        20% YIELD REDUCTION PER SUM06 EXPOSURE RESPONSE MODELS USED BY
1
VO












Ul
1
oo


M
u
i
g
0
s
O


LEEET
Experiment Chamber
A80SO- Corsoy NF+0.03-1
A83SO - Amsoy NF+0.03-1
A83SO - Corsoy NF+0.03-1
A85SO - Corsoy_79 D NFx2.00-lD
A85SO - Corsoy_79 W NFx2.00-lW
A86SO - Corsoy_79 D NFx2.5-lD
A86SO - Corsoy_79 W NFx2.0-lW
B83SO - Corsoy _79 D NF-1D
B83SO - Corsoy_79 W NF+0.03-1W
B83SO - Williams D NF+0.03-1D
B83SO - Williams W NF+0.03-1W
I81SO - Hodgson NF+0.06-1
R81SO - Davis NF-1
R82SO - Davis NF+0.02-1
R83SO - Davis Dry NF+0.02-1D
R83SO - Davis Wet NF+0.02-1W
R84SO - Davis Dry NF+0.015-1D
R84SO - Davis Wet NF+0.015-1W
R86SO - Young Dry NFxl .3- ID
R86SO - Young Wet NFxl .3-1 W
SORGHUM
A82SG - Dekalb NF+0.10-1
WHEAT

A82WH - Abe NF+0.03-1
A82WH - Arthur_71 NF+0.06-1
Min.
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000

0.000


0.000
0.000
10
0.000
0.001
0.001
0.000
0.000
0.002
0.002
0.002
0.002
0.002
0.002
0.004
0.003
0.001
0.002
0.002
0.006
0.006
0.003
0.003

0.001


0.002
0.002
AL. (1991) IN SELECTED
30
0.011
0.014
0.014
0.008
0.011
0.016
0.015
0.006
0.006
0.006
0.006
0.007
0.015
0.013
0.015
0.015
0.018
0.018
0.013
0.013

0.010


0.015
0.015
50
0.026
0.028
0.028
0.023
0.026
0.035
0.033
0.018
0.019
0.019
0.019
0.015
0.026
0.026
0.030
0.030
0.030
0.029
0.024
0.023

0.023


0.027
0.027
Percentiles
70 90
0.045
0.049
0.049
0.051
0.063
0.085
0.065
0.037
0.049
0.049
0.049
0.031
0.043
0.047
0.055
0.054
0.047
0.046
0.047
0.046

0.055


0.047
0.053
0.077
0.083
0.083
0.110
0.114
0.137
0.105
0.063
0.084
0.084
0.084
0.083
0.066
0.080
0.089
0.087
0.077
0.075
0.089
0.087

0.145


0.079
0.109
95
0.090
0.098
0.098
0.129
0.134
0.161
0.124
0.074
0.097
0.098
0.097
0.090
0.075
0.091
0.104
0.101
0.089
0.089
0.107
0.101

0.160


0.094
0.121
NCLAN EXPERIMENTS (ppm)
99
0.111
0.123
0.123
0.160
0.162
0.207
0.161
0.087
0.118
0.118
0.118
0.105
0.088
0.123
0.126
0.119
0.113
0.110
0.137
0.129

0.185


0.113
0.144
SUM
Number Number of Occurrences 06 08
Max ofObs. >0.06 S0.08 >0.10 (ppm-h)
0.123 1,344
0.168 1,992
0.168 1,992
0.194 2,352
0.199 2,352
0.279 2,040
0.242 2,040
0.111 1,512
0.135 1,512
0.137 1,512
0.135 1,512
0.132 1,680
0.145 2,664
0.203 2,160
0.155 2,640
0.138 2,640
0.140 2,496
0.159 2,496
0.206 2,568
0.198 2,568

0.223 2,040


0.149 1,344
0.170 1,344
263
467
467
657
729
784
719
184
359
364
359
323
421
471
721
698
512
486
597
573

599


300
373
113
223
223
495
547
654
510
51
198
204
198
191
79
218
378
359
208
193
345
323

557


130
293
35
90
90
319
358
515
271
5
70
66
70
29
6
56
163
140
59
62
175
136

516


43
186
21.1
39.16
39.1
67.5
75.1
92.1
69.6
13.5
30.1
30.5
30.1
26.7
30.2
39.0
61.6
58.7
41.2
38.9
53.7
50.2

79.1


24.1
37.4
10.7
22.1
22.1
56.2
62.5
83.2
55.1
4.4
18.9
19.5
18.9
17.4
7.0
21.4
37.7
35.0
19.9
18.6
36.2
32.8

76.3


12.5
31.8
W126
(ppm-h)
17.7
33.2
33.2
63.0
70.0
88.6
63.7
10.6
25.8
26.0
25.8
22.9
2.6
33.1
53.1
50.7
34.8
32.6
47.7
44.1

78.2


19.8
35.3

-------
TABLE 5-13 (cont'd). SUMMARY OF OZONE EXPOSURES THAT ARE CLOSEST TO THOSE PREDICTED FOR
           20% YIELD REDUCTION PER SUM06 EXPOSURE RESPONSE MODELS USED BY
1
£2 Experiment
A83WH - Arthur_71
BTI82WH - VONA
BTI83WH - VONA
CORN
A81MA - PAG 397
A81MA - Pioneer
COTTON
R82CO - Stoneville
R85CO (McNair) Dry
V R85CO (McNair) Wet
i— '
^> PEANUT
R80PN - NC-6
2 TOBACCO
3 R83TO - McNair 944
LEE ET AL. (1991)
Chamber
NF+0.06-1
NF-1
NF-1

NF +0.06-2
NF +0.06-2

NF-1
NFxl.99-lD
NFxl. 33-1 W

NF +0.015-1

NF +0.020-1
Min.
0.000
0.000
0.000

0.000
0.000

0.000
0.000
0.000

0.000

0.000
10
0.004
0.011
0.006

0.000
0.000

0.003
0.003
0.003

0.004

0.003
30
0.019
0.025
0.021

0.008
0.008

0.018
0.012
0.012

0.017

0.018
50
0.032
0.034
0.036

0.020
0.020

0.029
0.024
0.024

0.029

0.037
IN SELECTED
Percentiles
70 90
0.054
0.042
0.049

0.052
0.052

0.044
0.052
0.041

0.043

0.061
0.108
0.057
0.071

0.111
0.111

0.065
0.117
0.073

0.066

0.089
95
0.123
0.064
0.083

0.126
0.126

0.074
0.154
0.091

0.076

0.104
NCLAN EXPERIMENTS (ppm)
99 Max
0.159 0.186
0.072 0.098
0.097 0.116

0.150 0.187
0.150 0.187

0.087 0.152
0.221 0.291
0.129 0.166

0.091 0.112

0.121 0.155
Number
of Obs.
1,296
1,464
864

1,968
1,968

2,856
3,000
3,000

2,688

1,968
Number of Occurrences
>0.06 feO.08 aO.10
365
114
165

552
552

390
810
487

369

611
295
2
51

461
461

64
609
226

101

288
186
0
4

306
306

7
407
118

5

117
SUM
06 08
(ppm-h)
37.4
7.6
12.4

57.5
57.5

28.2
92.9
41.4

27.2

50.7
32.5
0.2
4.7

51.0
51.0

5.8
78.9
23.5

8.8

28.4
W126
(ppm-h)
35.6
6.2
9.8

55.1
55.1

22.7
88.2
35.9

22.0

42.6

-------
 1     with infrequent high hourly average concentrations (e.g., >0.10 ppm), might experience less
 2     yield reduction than predicted using NCLAN experimental results. For rural forest sites,
 3     21% (1987), 23% (1988), 54%  (1989), 50% (1990), and 52% (1991) of the sites exhibited
 4     3-mo cumulative SUM06 values greater than 24.4 ppm-h, but fewer than 11 hourly average
 5     concentrations equal to or greater than 0.10 ppm.  Tables 5-14 and 5-15 illustrate that sites
 6     that experience 3-mo, SUM06 values >24.4 ppm do not necessarily have peaks, whereas
 7     sites that experience values <24.4 ppm-h do have peaks.
 8          Krupa et al. (1993) tested  the importance of ambient O3 frequency distributions in
 9     eliciting a response  based on comparisons of non-filtered (NF) and charcoal-filtered (CF)
10     treatments using the NCLAN data.  Eight cases where yields in NF were significantly lower
11     than CF were matched with corresponding cases where the yields in CF and NF were not
12     significantly different.  The frequency distributions of NF treatments resulting in significant
13     yield loss had a greater proportion of concentrations >50 ppb than those of NF treatments
14     resulting in no significant yield  loss, indicating that these intermediate concentrations may
15     contribute to determining the magnitude of response. The authors conclude that
16     concentrations between 50 and  87 ppb are more important than concentrations > 100 ppb in
17     eliciting plant response. These conclusions are difficult to substantiate with the selected data
18     because:  (1) the NF treatments had few occurrences of concentrations > 100 ppb, and
19     consequently, the relative importance of peak concentrations > 100 ppb cannot be reliably
20     tested  with  any degree of statistical power; and (2) the  selected cases showing no significant
21     yield loss for NF do not closely match the cases showing significant yield loss for NF in
22     terms  of environmental conditions,  soil and nutrient condition, exposure periods and
23     durations,  sites, species and cultivars, and harvests (for clover studies).  Because these
24     factors interact with O3 effects  in determining plant response, differences in these factors
25     confound the comparison of frequency distributions  between cases having significant and
26     non-significant yield losses for  NF.  Another concern is the inconsistency of harvests for the
27     two clover studies conducted at Raleigh, NC, in 1984 and 1985, which have six and seven
 28      harvests, respectively (Heagle et al., 1989), not 12 as reported by Krupa et al. (1993).
 29           Reich (1987)  reviewed  44 studies on 45 species to study the effects of O3 on net
 30      photosynthesis (Pn) and growth of crops and tree species.   Plants responded differently to
 31      equivalent total exposures (i.e., SUMOO) when peak concentrations differed widely, with

        December  1993                           5-140      DRAFT-DO NOT QUOTE OR CITE

-------
TABLE 5-14.  SUMMARY OF PERCENTILES FOR OZONE MONITORING SITES IN 1989
1
BUT WITH SECOND
» » *. -•- .A.JL f. .m, A. *.•_(. m^ m_»_L V M. ^S ,i » M. JL. •*- .M_M.m. J -*f_^ ^V AV«rA ^ -*. M.M^ t*J WAV .», W T J. .B_M_* *t^l M-J ^** **~W«T I^MAJLl. MM.
HOURLY MAXIMUM CONCENTRATION .> 0.125 ppm
t . Maximum Number of Observ.
\O Percentiles
S












Ut
i
£



O
>
M
i.
O

o
H
O
d
AIRS Site
060010003
060371301
060374002
060375001
060830008
060830010
060833001
090010113
090091123
220191003
220330003
220330004
220331001
220470002
220770001
230052003
471630009
481410027
481990002
482010024
482010062
482011034
482011037
490350003
490353001



Name
LIVERMORE.CA
LYNWOOD,CA
LONG BEACH, CA
HAWTHORNE, CA
SANTA BARBARA, CA
SANTA BARBARA, CA
SANTA BARBARA CO, CA
BRIDGEPORT, CT
NEW HAVEN, CT
WESTLAKE, LA
BATON ROUGE, LA
BATON ROUGE, LA
E BATON ROUGE, LA
IBERVILLE PAR, LA
NEW ROADS, LA
CAPE ELIZABETH, ME
KINGSPORT, TN
EL PASO, TX
KOUNTZE, TX
HARRIS CO, TX
HOUSTON, TX
HOUSTON, TX
HOUSTON, TX
SALT LAKE CO, UT
SALT LAKE CITY, UT



Min.
.000
.000
.000
.000
.000
.000
.000
.000
.000
.000
.000
.000
.000
.000
.000
.001
.001
.000
.000
.000
.000
.000
.000
.000
.000



10
.000
.000
.010
.000
.010
.010
.010
.002
.003
.003
.001
.002
.003
.005
.001
.017
.001
.010
.000
.000
.000
.000
.000
.001
.002



30
.010
.010
.020
.020
.020
.020
.020
.011
.010
.013
.009
.008
.012
.014
.011
.027
.005
.020
.010
.010
.010
.010
.010
.008
.014



50
.030
.020
.020
.030
.030
.030
.030
.022
.019
.022
.021
.016
.022
.023
.021
.034
.017
.030
.020
.020
.020
.010
.010
.029
.029



70
.040
.030
.030
.040
.040
.040
.040
.033
.029
.033
.034
.028
.034
.034
.033
.042
.032
.040
.030
.030
.030
.030
.030
.042
.041



90
.050
.050
.050
.060
.050
.050
.050
.048
.045
.052
.059
.047
.056
.057
.052
.055
.054
.050
.050
.060
.050
.050
.050
.056
.053



95
.060
.070
.060
.060
.060
.060
.060
.059
.056
.061
.069
.057
.066
.068
.062
.064
.062
.060
.060
.070
.070
.060
.060
.062
.061



99
.090
.100
.080
.080
.080
.080
.080
.091
.091
.082
.094
.078
.092
.093
.083
.093
.078
.080
.080
.110
.110
.100
.110
.083
.079



Max.
.140
.140
.160
.190
.190
.220
.140
.156
.156
.137
.168
.138
.171
.149
.141
.146
.125
.260
.130
.230
.170
.220
.250
.125
.140



Uncorrected
SUM06 (ppm-h)
17.0
18.1
13.6
18.1
17.1
13.3
12.3
16.5
12.9
12.2
17.4
8.4
14.4
15.9
12.0
16.7
13.4
14.9
10.6
19.2
16.8
14.0
16.3
17.4
13.0



Over 7-mo
Period
5,067
4,793
4,876
4,894
4,823
4,663
5,077
4,865
4,502
4,811
4,964
4,791
4,890
5,040
4,964
4,627
4,252
4,484
4,630
4,728
4,600
4,595
4,729
4,585
4,544




-------
    TABLE 5-15. SUMMARY OF PERCENTILES FOR OZONE MONITORING SITES IN 1989
(APRIL THROUGH OCTOBER) WITH A MAXIMUM THREE-MONTH SUM06 VALUE > 24.4 ppm-h
1
fa
BUT WITH SECOND HOURLY MAXIMUM CONCENTRATION < 0.125 ppm











»T* Percentiles
S
W












i
§



d
§>
3
*p
d
> j
2!
H
O

0
O
AIRS Site
040132004
060070002
060170009
060430004
060710006
061011002
120094001
170190004
170491001
180970042
240030014
240053001
310550032
350431001
360310002
370270003
370810011
371470099
390030002
391510016
420070003
420770004
470090101
510130020
510610002
511870002
550270001
551390007


Name
SCOTTSDALE, AZ
CHICO, CA
SOUTH LAKE TAHOE, CA
YOSEMITE NP, CA
SAN BERNARDINO CO, CA
YUBA CITY, CA
COCOA BEACH, FL
CHAMPAIGN, IL
EFFDSfGHAM CO, DL
INDIANAPOLIS, IN
ANNE ARUNDEL, MD
ESSEX, MD
OMAHA, NE
SANDOVAL CO, NM
ESSEX CO, NY
LENOIR, NC
GUILFORD CO, NC
FARMVILLE, NC
ALLEN CO, OH
CANTON, OH
NEW BRIGHTON, PA
ALLENTOWN, PA
SMOKY MT NP, TN
ARLINGTON CO, VA
FAUQUIER CO, VA
SHEN NP (DKY RDG), VA
HORICON, WI
OSHKOSH, WI


Min.
.000
.000
.000
.000
.000
.000
.002
.000
.000
.001
.000
.000
.002
.000
.016
.000
.004
.000
.000
.000
.000
.000
.000
.000
.000
.004
.002
.002


10
.006
.010
.020
.008
.020
.000
.017
.008
.009
.006
.006
.002
.021
.010
.033
.007
.010
.010
.007
.008
.008
.003
.025
.001
.009
.027
.019
.016


30
.018
.020
.030
.022
.040
.020
.024
.020
.023
.021
.021
.010
.030
.020
.042
.019
.023
.023
.022
.019
.021
.016
.036
.010
.021
.037
.029
.028


50
.031
.030
.040
.035
.050
.030
.032
.029
.036
.034
.032
.024
.037
.030
.050
.032
.034
.034
.032
.030
.032
.028
.044
.023
.033
.045
.037
.038


70
.045
.040
.050
.049
.060
.040
.042
.039
.046
.046
.045
.038
.047
.040
.056
.045
.046
.044
.043
.042
.043
.039
.053
.037
.045
.054
.047
.048


90
.062
.060
.060
.065
.070
.060
.059
.065
.063
.063
.064
.059
.062
.060
.067
.062
.063
.062
.060
.060
.062
.060
.065
.059
.061
.065
.062
.063


95
.071
.070
.070
.072
.080
.070
.068
.072
.070
.072
.073
.069
.067
.060
.073
.067
.070
.070
.068
.070
.070
.070
.070
.071
.069
.071
.070
.070


99
.084
.080
.080
.083
.090
.080
.077
.078
.081
.085
.090
.089
.075
.070
.086
.078
.083
.083
.086
.088
.087
.087
.081
.088
.084
.082
.088
.084


Max.
AQ7
.100
.100
.111
.100
.100
.094
.088
.104
.103
.120
.121
.098
.090
.106
.092
.113
.100
.107
.110
.102
.102
.098
.116
.122
.100
.111
.121



Uncorrected
SUM06 (ppm-h)
— _

33.5
44.8
37.6
70.5
29.0
28.7
32.0
25.3
25.4
25.5
25.2
24.9
25.1
45.6
25.8
27.7
26.4
24.5
26.3
29.4
25.1
35.9
25.7
24.6
59.0
24.6
27.9



Over 7-mo
Period
5,070
4,690
4,768
4,853
4,856
4,623
5,012
5,091
4,600
4,592
4,360
5,028
4,160
5,059
4,070
4,806
4,853
4,833
4,854
4,875
5,055
5,040
4,764
5,029
5,050
4,454
4,142
4,206



-------
 1     greater loss of net photosynthesis (Pn) for increasing concentrations (Figure 5-15).  Short-
 2     term, high concentrations above 0.40 ppm (e.g., 0.50 ppm for 8 h) caused rapid and
 3     significant reduction in Pn. Longer-term exposures for weeks to lower concentrations had a
 4     significant effect on Pn; the observed reductions were less severe than at the higher
 5     concentrations.  Based on  short-term, high concentration studies, SUMOO alone was an
 6     inadequate descriptor of exposure for predicting response.  However, for assessing the effects
 7     of long-term, low concentrations typical of ambient condition, SUMOO may be adequate, as
 8     the response of field-grown plants to SUMOO was roughly linear.  SUMOO explained much,
 9     although not all, of the variation in net photosynthesis and growth  of conifers, hardwood
10     trees, and agricultural crops (Figures 5-16 through 5-18). Unexplained variation can be
11     attributed to biological variation, inherent experimental error, experimental conditions, and
12     differences in O3  uptake.  Imputed O3 uptake calculated as the product of SUMOO and mean
13     diffusive conductance (ks) for each species better correlated with Pn and growth than
14     SUMOO.
15          Kickert and Krupa (1991) criticized Reich's findings on the basis of  insufficient
16     reporting of statistical model parameters, possible non-normality of Pn and growth variables,
17     exclusion of ks terms for imputing O3 uptake for each species, and with no implication for
18     any individual plant species. However, Reich's synthesis of Pn and growth, using the
19     SUMOO index, would not necessarily be invalidated by non-normality of the variables and
20     provides evidence on the importance of peak concentrations and duration in eliciting a
21     response.  Reich's use of a mean diffusive conductance to impute O3 uptake is questionable
22     as leaf diffusive conductance measurements vary with time of day, season, and environmental
23     condition.  Consequently,  numerous measurements of conductance are required to weight
24     hourly O3  concentrations to calculate O3 uptake over the growth of a plant.
25          Pye (1988) reviewed  15 studies on 26 seedling species and found reductions in biomass
26     response increased with SUMOO  (Figure 5-19).  Seasonal sum of hourly concentrations
27     values ranged from 4 to 297 ppm-h.  However, there was substantial variation in response.
28     Pines, poplars,  sycamore,  ash, and maple are relatively sensitive.  Both concentration and
29     duration are important factors governing impact on growth and photosynthesis,  but they
30     probably are not equally important.  The biomass data suggest a nonlinear response to
       December 1993                          5.143      DRAFT-DO NOT QUOTE OR CITE

-------
       
-------
                        40      80      120
                            Dose (ppm-h)
  160
      10       20      30
        Uptake (mg/cm2)
                                                                                        40
       Figure 5-16.  Percent reduction in net photosynthesis and biomass growth of coniferous
                    species in relation to (a) total exposure (SUMOO) and (b) estimated total
                    ozone uptake (Reich, 1987).
 1     fumigation and the presence of convexity of response implies that for similar mean
 2     O3 exposures, damage will be greater when O3 concentrations are more variable.
 3          There is limited information for assessing the relative performance of exposure indices
 4     for relating to vegetation effects.  Lefohn et al. (1992a) reported that it was not possible to
 5     differentiate among the SUMOO, SUM06, W126, and SUM08 exposure indices because the
 6     indices were highly correlated with one another in the experiment (Figure 5-20).  However,
 7     results based on biological experiments,  reported by Musselman et al. (1983) and Hogsett
 8     et al.  (1985a) have shown that different exposure regimes with similar SUMOO values
 9     resulted in those exposures experiencing capture peak concentrations exhibiting the greater
10     effects.  The authors demonstrated that plants exposed to variable concentrations showed
       December 1993
5-145
DRAFT-DO NOT QUOTE OR CITE

-------
            20
                     20    40    60    80   100   120
                            Dose (ppm-h)
                10     20    30     40
                    Uptake (mg/cm2)
                               so
       Figure 5-17. Percent reduction in net photosynthesis and biomass growth of hardwood
                   species in relation to (a) total exposure (SUMOO) and (b) estimated total
                   ozone uptake (Reich, 1987).
 1      greater effect on plant growth than those exposed to a fixed or daily peak concentration of
 2      equal SUMOO but lower peak concentrations.
 3          Building upon the above cited results that biologically showed that the importance of
 4      the higher hourly average concentrations, Lefohn et al. (1989) concluded that the SUMOO
 5      index did not appear to perform adequately.  Using air quality data, Lefohn et al.  (1989)
 6      showed that die magnitude of the SUMOO exposure index was largely determined by the
 7      lower hourly average concentrations instead of the biologically relevant higher hourly
 8      average concentrations (Figure 5-21).  Figure 5-21 illustrates that the slope of the curve that
 9      described the cumulative frequency for the SUMOO index (referred  to as TOTDOSE) was
10      greater than the slope of the curve for the W126 index until approximately 0.06 ppm.
       December 1993
5-146
DRAFT-DO NOT QUOTE OR CITE

-------
        <£   -20
        c
        o
       O
-40

-60

-80
  C

20

 0

-20

-40

-60

-80
                      10
                                           Crops
      20

      0

      -20 \

      -40

      -60

      -80
Crops
                    20    40    60    80    100    120
                           Dose (ppm-h)
                10     20     30     40
                    Uptake (mg/cm2)
      so
      Figure 5-18. Percent reduction in net photosynthesis and biomass growth of agricultural
                   crops in relation to (a) total exposure (SUMOO) and (b) estimated total
                   ozone uptake (Reich, 1987).
1     Thereafter, the reverse was true.  This occurred because the W126 index weighted the higher
2     concentrations more heavily than the lower ones, while the TOTDOSE index did not.
3          Supplementing the results in Lefohn et al. (1989), Lefohn et al. (1992a), using loblolly
4     pine data exposed at Auburn, AL, to varying levels of O3 over 555 days (Qiu et al., 1992)
5     reported that the magnitude of the SUMOO values in the CF chamber, although experiencing
6     hourly average values greater than those at the South Pole or Pt. Barrow, AK, was about
7     50% less than the SUMOO values experienced at the South Pole and Pt. Barrow, AK.
8          In a  similar analysis using ambient data, Lefohn et al. (1992a) identified a separate set
9     of ambient sites that experienced SUMOO values similar to those of the ambient treatments at
      December 1993
5-147      DRAFT-DO NOT QUOTE OR CITE

-------
          50

          25
       5-25
       c
       6
          -75
        -100

                                                                                 !F
                                                             ft
              0      25    50     75   100   125   150   175   275  300
                                 Ozone Exposure (nil1 hr)
      Figure 5-19.  Percent reduction in biomass growth of tree seedlings in relation to total
                   exposure (Pye, 1988).
 1     Auburn; these ambient sites experienced fewer hourly concentrations above 0.07 ppm than
 2     did the ambient chambers. Similar to the results cited above, the authors noted that the
 3     magnitude of the SUMOO index was unable to capture the occurrence of the higher hourly
 4     average concentrations in the ambient treatments.  The authors indicated that the SUMOO
 5     index was inadequate because of the observed inconsistences of the SUMOO value between
 6     chambers and selected monitoring sites.
 7          When taken by themselves, the importance of these findings may be debatable because
 8     the clean sites  are not representative of loblolly growing regions and there is no
 9     substantiating evidence of differing effects at these levels. However, the coupling of the air
10     quality considerations, as described by Lefohn et al. (1989, 1992a), with the biological
       December 1993
5-148
DRAFT-DO NOT QUOTE OR CITE

-------
1
£,0.8
CM
fo.e
|°-4
< 0.2
°(
a)
o 2*0.8
CM
T3
o £°'6
o ®
x w 0.4
X 3
x < 0.2
c)
o

o
o
X
X
X
) 100 200 300 400 500 600 700 °0 100 200 300 400 500 600 70
                     SumO (ppm-h)
                Sum06 (ppm-h)
1
~0.8:
CM
•o
C0.6'
^J
§0.4
3
xT
<0.2
f\
b)
£-°-8>
CM
s, ,
^0.6'
o ~~
•o
|0.4
x 3
^
<0.2
d)
o


o
i
X
X

'
            '0  100 200 300 400 500 600 700
                      w126 (ppm-h)
       '0  100  200 300 400 500 600 700
                 SumOS (ppm-h)
      Figure 5-20.  Reduction in volume production of loblolly pine seedlings (family 91) in
                  relation to four exposure indices (a-d) (Lefohn et al., 1992a).
1     findings reported by Musselman et al. (1983) and Hogsett et al. (1985a), builds a consistent
2     picture that the SUMOO index does not properly describe the occurrence of the higher hourly
3     average concentrations.
      December 1993
5-149
DRAFT-DO NOT QUOTE OR CITE

-------




^
0)
1
«v

0)
3s
3
E
=»
O






1.0
0.9
0.8

0.7

0.6

0.5

0.4


0.3
0.2

0.1

n n
\j.\j
I l t I I I I I I I I I
A W126 0 • A A A
* Both * A
• A A
A
-
A
•
A

~~ •
A

^
"A
•
A
• A
• A
A
I 1 I I I I I I I I I I
                  0.00 0.01   0.02 0.03  0.04  0.05  0.06  0.07  0.08  0.09  0.10  0.11  0.12
                                              Level (ppm)
      Figure 5-21.  A comparison between the resulting cumulative frequencies for the
                   exposure parameters (a) sum of all hourly average concentrations (SUMOO)
                   and (b) the sigmoidally weighted integrated exposure index, W126. The
                   ozone data were collected in 1981 at a site located in the Mark Twain
                   National Forest, Missouri. The U.S. EPA AIRS site number is 291230001
                   (Lefohn et al., 1989).
1          The selection of the weighting scheme of hourly O3 concentrations for use in
2     characterizing plant exposure and its relationship to plant response is difficult because of
3     limitations in the data.  The results of studies based on analysis of experimental and air
4     quality data substantiate O3 uptake as the determining factor of response.  Stomata controls
5     the rate of O3 uptake.  Stem et al. resistance is influenced by ambient conditions surrounding
6     the plant, as well as other factors. Concentration has been identified as important in
7     predicting response and concentrations as low as 50 ppb may contribute to response. Several
8     lines of evidence suggest that the peak-weighted, cumulative indices yield better predictions
       December 1993
5-150
DRAFT-DO NOT QUOTE OR CITE

-------
 1     of yield loss than the mean and peak indices.  The optimal weighting function to describe
 2     plant exposure has not been determined but should give greater weight to the peak
 3     concentrations.  Because the NCLAN studies used ambient-added exposures that have
 4     considerably more concentrations above 0.10 ppm than ambient conditions in polluted
 5     monitoring sites, one must be careful in the selection of an exposure index based on
 6     statistical fit.
 7
 8     5.5.3    Summary
 9          The effects of O3 on individual plants and factors that modify plant response to O3 are
10     complex and vary with factors, such as species, environmental conditions, and soil and
11     nutrient conditions. Because of the complex effect of O3 and its interactions with physical
12     and genetic factors that influence response, it is difficult to develop a measure of exposure
13     that  relates well with plant response based on experimental data.  At best, experimental
14     evidence of the impact of  O3 on biomass  production can indicate important factors of
15     O3 exposure that  modify plant response, which become considerations in developing  an
16     exposure index.
17          Considerable evidence of the primary mode of action of O$  on plants (injury to proteins
18     and membranes, reduction in photosynthesis, changes in allocation of carbohydrate, and early
19     senescence), which ultimately lead to reductions in biomass production, identifies O3 uptake
20     as an important factor (see Section 5.2).  Ozone uptake is controlled by canopy conductance,
21     stomatal conductance, and O3 concentration outside the leaf (see Figure 5-2).  Any factor
22     that  will affect  stomatal conductance (e.g., light, temperature, humidity, soil and atmospheric
23     chemistry and nutrients, time of day, phenology, and biological agents) will affect Oj uptake
24     and, consequently plant response.
25          Evidence  from studies that applied two or more different exposure regimes substantiate
26     the importance of daytime peak concentrations,  respite time, and phenology in eliciting a
27     response.   Ozone effects on plants exposed to two (or more) regimes  having equal total
28     exposure were greater for exposures experiencing the higher peak concentrations, respite
29     time of 2 to 6 days, or peak concentrations during period of maximum leaf expansion, This
30     conclusion is consistent with the mode of action of O3 on plants and with the conclusions in
31     the previous Environmental Protection Agency criteria document (U.S. Environmental

       December  1993                          5.151      DRAFT-DO NOT QUOTE OR CITE

-------
 1     Protection Agency, 1986) and its Supplement (U.S. Environmental Protection Agency, 1992)
 2     and is equally true for seedlings based on a recent seedling study (Hogsett and Tingey,
 3     1990).
 4           Further, the biochemical mechanisms, discussed in Section 5.2, describe the mode of
 5     action of O3  on plants as the culmination of a series of physical, biochemical, and
 6     physiological events leading to alterations in plant metabolism.  Ozone-induced injury is
 7     cumulative, resulting in net reductions in photosynthesis, changes in allocation of
 8     carbohydrate, and early senescence,  which lead to reductions in biomass production
 9     (Section 5.2).  Increasing O3 uptake will result in increasing reductions in biomass
10     production.  Retrospective analyses comparing replicate studies of equal and varying
11     durations are in general agreement that the ultimate impact of 03 on plant response depends
12     upon the integration of repeated peak concentrations during the ecological period of growth.
13           The optimum exposure index that relates well with plant response should incorporate
14     the factors (directly or indirectly) described above; unfortunately, such an index has not yet
15     been identified. At this time, exposure indices that weight the  hourly O3 concentrations
16     differentially appear to be the best candidates for relating  exposure  with predicted plant
17     response.  Peak concentrations in ambient air occur primarily during daylight thus, these
18     indices, by providing preferential weight to the peak concentrations, give greater weight to
19     the daylight  concentrations rather than nighttime concentrations (when stomatal conductance
20     is minimal).
21           Studies reported in the literature show that when O3 is the primary source of variation
22     in response, year-to-year variations  in plant response are minimized by the peak-weighted,
23     cumulative exposure indices. The data suggest that the exposure indices that cumulate hourly
24      O3 concentrations over the growing season and  give preferential weight to the peak
25      concentrations are biologically appropriate as characterizations and representations of plant
26      exposure.  Generally, the peak-weighted, cumulative indices rekte well with plant response
27      and order the treatment means in monotonically decreasing fashion with increasing exposure,
 28      based on studies that apply two or more types of exposure regimes and when combining data
 29      from replicate studies of the same species.  No studies have been designed specifically to
 30     evaluate the adequacy of the peak-weighted, cumulative indices.  Consequently, it is  not
 31      possible to discriminate among the various peak-weighted, cumulative indices based on

        December 1993                           5-152     DRAFT-DO NOT QUOTE OR CITE

-------
 1     experimental data.  Functional weighting approaches including an allometric, sigmoid, or
 2     threshold weighting have been suggested and, in earlier retrospective studies compared, but
 3     there is no evidence to favor one approach over the other on the basis of statistical fits to the
 4     data.
 5           The study of Fuhrer et al. (1992) illustrates some of the limitations in applying
 6     exposure indices.  The study is significant for its use of the mean O3 flux in minimizing the
 7     year-to-year variation in response when combining replicate studies, indicating the
 8     importance of environmental conditions in quantifying the relationship between O3 exposure
 9     and  plant response.
10           The factors such as respite time, temporal variation, phenology, canopy structure,
11     physiological processes, environmental conditions,  and soil and nutrient conditions, are
12     important in determining the impact of O3 on crops and trees but are not well understood and
13     interact with concentration and duration in different fashions depending upon species. Ozone
14     uptake integrates these factors with atmospheric conditions, relates well with plant response,
15     but is difficult to measure. Empirical functions to  predict stomatal conductance have been
16     developed for particular species (e.g., Losch and Tenhunen, 1981)  but have not been used to
17     estimate O3 uptake or used in  development of exposure indices.
18           The exposure-response studies in the published literature support the conclusion that
19     O3 effects are cumulative and  peak concentrations are more important than lower
20     concentrations in determining  the magnitude of plant response.  The peak-weighted,
21     cumulative indices appear to have major advantages over the mean (e.g., 7-h seasonal mean),
22     peak indices (e.g., 2ndHDM), and the index that cumulates all hourly average concentrations
23     (i.e., SUMOO).  Crop yield loss and biomass reduction are better estimated using the peak-
24     weighted, cumulative indices than the 2ndHDM index; when duration of exposure is taken
25     into consideration, peak-weighted cumulative indices perform better than the seasonal mean
26     indices.  In addition, results have been published to indicate that the SUMOO index does not
27     adequately relate exposure with biological effects because the index focuses on the lower
28     hourly average concentrations.
29           For predicting the effects of O3 on vegetation under ambient conditions using
30     experimental exposure-response models, the  types of exposure regimes used in the
31     experiments should be taken into consideration. For example, NCLAN experiments

       December  1993                          5.153      DRAFT-DO NOT QUOTE OR CITE

-------
 1     contained peak hourly average concentrations in their regimes.  Any exposure index, based
 2     on the NCLAN experiments, should take into consideration the presence of these peak
 3     concentrations.  By doing so, the situation may be avoided where two sites, which experience
 4     two distinct distributions of high hourly average concentrations, but have the same value of
 5     cumulation (e.g., same SUM06 or W126 value), exhibit differing biological effects.
 6          Future research needs to focus on:  (1) validation of the application of exposure-
 7     response relationships based on chambered studies to ambient conditions; (2) evaluation of
 8     peak-weighted, cumulative indices for quantifying the relationship of O3 exposure to ensuing
 9     plant response; (3) a better understanding of the effects of O3 and its interactions with
10     environmental conditions, soil chemistry, and nutrient conditions; (4) development of
11     mechanistic models of stomatal conductance for use in weighting O3 concentrations in
12     ambient air; and (5) more multi-year exposure studies on trees to predict the long-term
13     effects on O3 of biomass production.
14
15
16     5.6    EXPOSURE-RESPONSE OF PLANT SPECIES
17     5.6,1    Introduction
18          Determining the response of plants to O3 exposures continues to be a major challenge.
19     The effects of vegetational exposure are usually evaluated by exposing various plant species
20     under controlled experimental conditions such as those discussed in Section 5.2. Plant
21     responses are influenced not only by the biochemical and physiological changes that may
22     occur within  the plant after O3 entry (Section 5.3, Mode of Action, see also Figure 5-5) but
23     also by the many  factors that modify plant response (Section 5.4).  Of the factors  discussed
24     in Section 5.4,  those that are most likely to apply under controlled experimental conditions
25     are the genetic  makeup and age of the plant.  Compensatory responses (Section 5.3.4.2) will
26     also influence plant response.  This section will analyze, summarize, and evaluate what is
27     known about the response of various plant species or cultivars, either as an individuals or in
28     populations to O3 exposure.  Species as populations will only be considered in the case of
29     pasture grasses, or  forage mixes, which commonly occur as mixed stands. Emphasis will be
 30     placed on those studies conducted since the publication of the previous criteria document
 31      1986 (U.S. Environmental Protection Agency, 1986). Much of the discussion of  vegetational

        December 1993                          5-154     DRAFT-DO NOT QUOTE OR CITE

-------
 1     response to O3 exposure in the current document is based on the conclusions of both the
 2     1978 and 1986 documents (U.S. Environmental Protection Agency,  1978,  1986).  Therefore,
 3     to provide a basis for understanding the effects presented below, the conclusions of the two
 4     documents are summarized.
 5          Finally, the results of O3 exposure-response presented  in this section must be related to
 6     one or more assessment endpoints. Historically, the dollar value of lost production was the
 7     endpoint of interest, however, other endpoints (e.g., biodiversity, habitat,  aesthetics,
 8     recreation) must be considered now, particularly as the impacts of O3 on long-lived species
 9     of ecological importance are evaluated (Tingey et al., 1990).
10
11     5.6.2  Summary of Conclusions from the Previous Criteria  Documents
12          The experimental data presented in the 1978  and 1986 criteria documents dealt with the
13     effects of O3 primarily on agricultural crops species (U.S. Environmental  Protection Agency,
14     1978, 1986). The chapter on vegetational effects in the 1978 criteria document (U.S.
15     Environmental Protection  Agency, 1978)  emphasized visible injury and growth effects;
16     however, the growth effects  were not those that affected yield. This emphasis was dictated
17     by the kind of data available at the time.  The document also presented data dealing with the
18     response of the San Bernardino ecosystem to O3.  This information was also discussed in the
19     1986 document (U.S. Environmental Protection Agency, 1986). It remains the best study of
20     ecosystem responses to O3 stresses (see Section 5.7).
21          The 1986 document  emphasized the fact that though foliar injury on vegetation  is one
22     of the earliest and most obvious manifestations of O3 exposure, the effects of exposure are
23     not limited to visible injury.  Plant foliage is only  the primary site of plant response to
24     O3 exposures. Significant secondary effects, include reduced growth, both in foliage  and
25     roots.  Impacts range from reduced plant growth and decreased yield to changes in crop
26     quality and alterations  in plant susceptibility to biotic and abiotic stresses.   Also, the  1986
27     document noted that O3 exerts a phytotoxic effect  only if a sufficient amount reaches
28     sensitive sites within the leaf (see Section 5.3).  Ozone injury will not occur if (1) the rate of
29     uptake is low enough that the plant can detoxify or metabolize O3 or its metabolites;  or
30     (2) the plant is  able to repair or compensate for the effects (Tingey and Taylor, 1992; U.$.
31     Environmental  Protection  Agency, 1986). Cellular disturbances that are not repaired or

       December 1993                          5-155      DRAFT-DO NOT QUOTE OR CITE

-------
 1     compensated are ultimately expressed as visible injury to the leaf or as secondary effects that
 2     can be expressed as reduced root growth, or reduced yield of fruits or seeds, or both.  Ozone
 3     would be expected  to reduce plant growth or yield if (1) it directly impacts the plant process
 4     e.g.,  photosynthesis that was limiting plant growth; or (2) it impacts another step sufficiently
 5     so that it becomes the step limiting plant growth (U.S. Environmental Protection Agency,
 6     1986; Tingey,  1977).  Conversely, if the process impacted is not or does not become rate-
 7     limiting, O3 will not limit plant growth. These conditions also suggest that there are
 8     combinations of O3 concentration and exposure duration that a plant can experience that will
 9     not result in visible injury or reduced plant growth and yield. Indeed, numerous studies have
10     demonstrated this fact.  This information is  still pertinent today (Section 5.3)
11           Ozone can induce a diverse range of effects beginning with individual plants and then
12     proceeding to plant populations and ultimately  communities. The effects may be classified as
13     either (1) injury or (2) damage. Injury encompasses all plant reactions such as reversible
14     changes in plant metabolism (e.g., altered photosynthesis), leaf necrosis, altered plant
15     quality,  or reduced growth that does not impair yield or the intended use or value of the
16     plant (Guderian, 1977).  Thus, for example, visible foliar injury to ornamental plants,
17     detrimental responses in native species, while reductions in fruit and grain production in
18     cultivated plants are all considered damage or  yield loss.  Although foliar injury is not
19     always classified as damage, its occurrence indicates that phytotoxic concentrations of O3 are
20     present and, therefore,  studies should be conducted to assess the risk to vegetation.
21           The concept of limiting values used to summarize visible foliar injury in the 1978
22     document was also considered valid in the 1986 document (U.S. Environmental Protection
23     Agency, 1978, 1986).  Jacobson, (1977) developed limiting values by reviewing the scientific
24     literature and identifying the lowest concentration and exposure duration reported to cause
25      visible injury to a  variety of plant  species.  Expressed  in another way, limiting values were
26      concentrations and durations of exposure below which  visible injury did not occur.
27      A graphical analysis presented in both of the previous  documents indicated the limit for
28      reduced plant performance was an exposure to 0.05 ppm for several hours per day for
 29      greater than 16 days. Decreasing  the exposure period  to 10 days increased the concentration
 30      required to cause injury to 0.1 ppm, and a  short, 6 day exposure further increased the
 31      concentration to cause injury to 0.30 ppm.

        December 1993                           5-156      DRAFT-DO NOT QUOTE OR CITE

-------
 1          By 1986, a great deal of new information concerning the effects of O3 on the yield of
 2     crops plants had become available, both through the EPA National Crop Loss Assessment
 3     Network (NCLAN) and the results of research funded by other agencies.  The NCLAN
 4     project was initiated by  the Environmental Protection Agency in 1980 primarily to improve
 5     estimates of yield loss in the field and to estimate the magnitude of crop losses caused by
 6     O3 (Heck et al., 1982).  The primary objectives were:
 7
 8          1.  To define the relationships between yields  of major agricultural crops and
 9              O3 exposure  as required to provide data necessary for economic assessments and the
10              development  of National Ambient Air Quality Standards;
11
12          2.  To assess the national economic consequences resulting from the exposure of major
13              agricultural crops to O3;
14
15          3.  To advance understanding of the cause and effect relationships that determine crop
16              responses to  pullutant exposures.
17
18          The cultural conditions used in the NCLAN studies approximated typical agronomic
19     practices.  The methodology used in these studies is described in Section 5.2.
20          Yield loss in the 1986 document was defined  as an impairment in the intended  use of
21     the plant.  This concept included reductions in aesthetic values, the occurrence of foliar
22     injury (changes in plant appearance), and losses in  terms of weight, number, or size of the
23     plant part that is harvested.  Yield loss may also include changes in physical appearance,
24     chemical composition, or the ability to withstand quality storage; which collectively are
25     termed  crop quality.  Losses  in aesthetic values are difficult to quantify. Foliar injury
26     symptoms can substantially reduce the marketability of ornamental plants or crops in which
27     the foliage is the plant part (e.g.,  spinach, lettuce,  cabbage) and constitute yield loss with or
28     without concomitant growth reductions.  At that time (1986) most studies of the relationship
29     between yield loss and O3 concentration focused on yields as measured by weight of the
30     marketable organ of the plant.
31          Open-top field chamber studies conducted to estimate the impact of O3 on the yield of
32     various crops species, e.g., the NCLAN program,  were grouped into two types, depending
33     on the experimental design and statistical methods used to a analyze the data:  (1) studies that
34     developed predictive equations relating O3 exposure to plant response, and (2) studies that

       December 1993                            5_157      DRAFT-DO NOT QUOTE OR CITE

-------
 1     compared discrete treatment level to a control.  The advantage of the regression approach is
 2     that exposure-response models can be used to interpolate results between treatment levels (see
 3     Section 5.2.2).
 4          Using NCLAN data as an example of plant response, the O3 concentrations that could
 5     be predicted to cause  10 or 30% yield loss were estimated using the Weibull function
 6     (Table 5-16; Table 6-19, U.S. Environmental Protection Agency, 1986). The data in
 7     Table 5-16 are based on yield-response functions for 38 species or cultivars developed from
 8     studies using open-top chambers.  Review of that data indicated that ten percent yield
 9     reductions could be predicted for 57% of the species or cultivars when 7-h seasonal mean
10     concentrations were below 0.05 ppm, for 35 %  when seasonal mean concentrations were
11     between 0.04 and 0.05 ppm, but only 19% required a 7-h seasonal mean concentrations in
12     excess of 0.08 ppm to suffer a 10% loss in yield. Furthermore, approximately 11% of the
13     38 species or cultivars would be expected to have a yield reduction of 10% loss at 7-h
14     seasonal mean concentrations below 0.05 ppm, suggesting that these plants are very sensitive
15     to O3.
16           Grain crops were  apparently less sensitive than the other crops.  The data also
17     demonstrate that the sensitivity within species may be as great as difference between species.
18     For example,  at 0.04 ppm O3, estimated yield  losses ranged from 2 to 15% in soybean and
19     from 0 to 28% in wheat.  Year to year variations in plant response were also observed
20     during the studies.
21           Discrete treatments were used to determine yield loss  in some studies.  These
22     experiments were designed to test whether specific O3 treatments were different from the
23     control rather than to develop exposure-response equations  and the data were analyzed using
24     analyses of variance. When summarizing these studies using discrete treatment levels, as
25     opposed to the variable concentrations used  in NCLAN, the lowest O3 concentration that
26      significantly reduced yield was determined from analyses done by the authors. Frequently,
27      the lowest concentration used in the study was the lowest concentration reported to reduce
28      yield; hence it was not always possible to estimate a no-effect exposure concentration.
29      In general, the data indicated that O3 concentrations of 0.10 ppm (frequently the  lowest
 30      concentration used  in the  studies) for a few  hours per day for several days to several weeks
        December 1993                          5-158      DRAFT-DO NOT QUOTE OR CITE

-------
 TABLE 5-16. ESTIMATES OF THE PARAMETERS FOR FITTING THE WEffiULL
 MODEL USING THE 7-HOUR SEASONAL MEAN OZONE CONCENTRATIONS*'*
                         Parameters for Weibull Model
                        Concentration for
                        Predicted Yield
                          Losses of:
Crop
LEGUME CROPS
Soybean, Corsoy
Soybean, Davis (81)
Soybean, Davis (CA-82)"
Soybean, Davis (PA-82)C
Soybean, Essex (81)
Soybean, Forrest (82-1)
Soybean, Williams (81)
Soybean, Williams (82-1)
Soybean, Hodgson
Bean, Kidney (FP)f
Peanut, NC-6
GRAIN CROPS
Wheat, Abe (82)
Wheat, Arthur 71 (82)
Wheat Roland
Wheat, Vona
Wheat, Blueboy n (T)
Wheat, Coker 47-27 (T)
Wheat, Holly (T)
Wheat, Oasis (T)
Corn, PAG 397
Corn, Pioneer 3780
Corn, Coker 16 (T)
Sorghum, DeKalb-28
Barley, Poco
FIBER CROPS
Cotton, Acala SJ-2 (81-1)
Cotton, Acala SJ-2 (82-1)
Cotton, Stoneville
HORTICULTURAL
CROPS
Tomato, Murrieta (81)
Tomato, Murrieta (82)
Lettuce, Empire (T)
Spinach, America (T)
Spinach, Hybrid (T)
Spinach, Viroflay (T)
Spinach, Winter Bloom (T)
A
a

2785.00
5593.00
4931.00
4805.00
4562.00
4333.00
4992.00
5884.00
2590.00
2878.00
7485.00

5363.00
4684.00
5479.00
7857.00
5.88
5.19
4.95
4.48
13968.00
12533.00
240.00
8137.00
1.99

5546.00
5872.00
3686.00


32.90
32.30
1245.00
21.20
36.60
41.10
20.80
A
a

0.133
0.128
0.12/
0.103
0.187
0.171
0.211
0.162
0.138
0.120
0.111

0.143
0.148
0.113
0.053
0.175
0.171
0.156
0.186
0.160
0.155
0.221
0.296
0.205

0.199
0.088
0.112


0.142
0.082
0.098
0.142
0.139
0.129
0.127
A
c

1.952
0.872
2.144
4.077
1.543
2.752
1.100
1.577
1.000
1.171
2.249

2.423
2.154
1.633
1.000
3.220
2.060
4.950
3.200
4.280
3.091
4.460
2.217
4.278

1.228
2.100
2.577


3.807
3.050
1.220
1.650
2.680
1.990
2.070
CP

0.022
0.025
0.019
0.019
0.014
0.017
0.014
0.017
0.017
0.019
0.025

0.023
0.023
0.023
0.022
0.030
0.030
0.030
0.030
0.015
0.015
0.020
0.016
0.020

0.018
0.012
0.026


0.012
0.012
0.043
0.024
0.024
0.024
0.024
10%d

0.048
0.038
0.048
0.059
0.048
0.076
0.039
0.045
0.032
0.033
0.046

0.059
0.056
0.039
0.028
0.088
0.064
0.099
0.093
0.095
0.075
0.133
0.108
0.121

0.044
0.032
0.047


0.079
0.040
0.053
0.046
0.043
0.048
0.049
30%d

0.082
0.071
0.081
0.081
0,099
0.118
0.093
0.088
0.066
0.063
0.073

0.095
0.094
0.067
0.041
0.127
0.107
0.127
0.135
0.126
0.111
0.175
0.186
0.161

0.096
0.055
0.075


0.108
0.059
0.075
0.082
0.082
0.080
0.080
December 1993
5-159     DRAFT-DO NOT QUOTE OR CITE

-------
         TABLE 5-16 (cont'd).  ESTIMATES OF THE PARAMETERS FOR FITTING THE
               WEIBULL MODEL USING THE 7-HOUR SEASONAL MEAN OZONE
         	                      CONCENTRATIONS^	
                                                                                 Concentration for
                                                                                  Predicted Yield
                                         Parameters for Weibull Model                   Losses of:
Crop
Turnip, Just Right (T)
Turnip, Pur Top W.G. (T)
Turnip, Shogoin (T)
Turnip, Tokyo Cross (T)
at
10.89
6.22
4.68
15.25
a
0.090
0.095
0.096
0.094
c
3.050
2.510
2.120
3.940
CP
0.014
0.014
0.014
0.014
10%"
0.043
0.040
0.036
0.053
30%"
0.064
0.064
0.060
0.072
        Data are from Heck et al. (1984b) and are based on individual plot means unless the crop name is followed by
        "(T)".  The "T" indicates that the parameters were based on treatment means and the data are from Heck et al.
        (1983a). The parameters given in Heck et al. (1983a, 1984b) also contain the standard errors of the
        parameters.
        All estimates of  a are in ppm. The yield is expressed as kg/Ha for all crops except barley—see weight (g per
        head); tomato (both years)—fresh weight jlcg per plot); cotton—lint + seed weight (kg/ha); peanut—pod weight
        (kg/Ha). In cases where the estimated  c parameter is exactly 1.0, it has been bounded from below to obtain
        covergence in the nonlinear model fitting routine.  Parameters were estimated from data not showing the
        expected Weibull form.  Caution should be used in interpreting these Weibull models.  Other models might
        better describe the behavior observed in these experiments. For those crops whose name is followed by "(T)"
        the yield is expressed as g/plant.
       °The 03 concentration in the charcoal filtered chambers expressed as a 7-h seasonal  mean concentration.
        The 7-h seasonal mean O3 concentration (ppm) that was predicted to cause a 10 or  30% yield loss
        (compared to charcoal-filtered air).
       eCA and PA refer to constant and proportional O3 addition.
        Only the bean data from the full plots are shown.  The partial plot data are given Heck et al. (1984b).

       Source: U.S. Environmental Protection Agency (1986).
 1      generally caused significant yield reductions.  The concentrations derived from the
 2      regressions studies were based on a 10% yield loss, while in the studies using the analysis of
 3      variance the 0.10 concentration frequently induced  mean yield losses of 10 to 50%.
 4           A chemical protectant, ethylene diurea (EDU) was used to provide estimates of yield
 5      loss.  The impact of O3 on yield was determined by comparing the yield data from plots
 6      treated with EDU  with those that were not.  Studies indicated that yields were reduced by
 7      18 to 41 % when ambient 63 concentrations exceeded 0.08 ppm during the day for 5 to
 8      18 days  over the growing season.
 9           In  summary, the  1986 criteria document (U.S. Environmental Protection Agency, 1986)
10     states  that the following several  general conclusions can be drawn from the various
11      approaches used to estimate crop loss yield; (1) Based on the comparison of data obtained

       December 1993                           5-160      DRAFT-DO NOT QUOTE OR CITE

-------
 1     from crop yield in charcoal-filtered and unfiltered (ambient) exposures clearly indicate that
 2     O3 at ambient levels are sufficiently elevated in several parts of the country to impair the
 3     growth and yield of plants.  This conclusion is supported by data from the chemical
 4     protectant studies and extends it to other plant species;  (2) Both of the above mentioned
 5     approaches indicate that effects occur with only a few O3 occurrences above 0.08 ppm;
 6     (3) The growth and yield data cited in the 1978 criteria document (U.S. Environmental
 7     Protection Agency, 1978) indicate  that  several plant species exhibited growth and yield
 8     effects when  the mean O3 concentration exceeded 0.05 ppm for 4 to 6 h/day for at least
 9     2 weeks; and (4) The data obtained from  regression studies conducted to develop exposure-
10     response functions for estimating yield  loss indicated that at least 50% of the species/cultivars
11     tested were predicted to exhibit a 10%  yield loss at 7-h season mean O3 concentrations of
12     0.05 ppm or less. Though most of the data from the discrete treatment studies did not use
13     concentrations low enough to support the values cited above, the magnitude of yield  losses
14     reported at 0.10 ppm under a variety of exposure regimes indicate that to prevent O3 effects
15     a substantially lower concentration is required.
16          The limiting values established in the 1978 were still deemed appropriate in the 1986
17     criteria document for ornamentals and certain vegetable crops where visible injury was still
18     considered the response of interest because appearance is of importance (e.g., spinach,
19     lettuce, cabbage) (U.S. Environmental  Protection Agency, 1986). This remains the  case
20     today.
21
22     5.6.3   Information in the Published Literature Since 1986
23          The major question to be addressed in this section is whether the conclusions of the
24     1986 criteria document summarized in  the previous section, remain valid given the results of
25     research published since  1988.  In particular, whether the response of plants to experimental
26     treatments at or near concentrations of 0.05 ppm (7 h seasonal mean), characteristic  of
27     ambient concentrations in many  areas,  can be compared to a control,  or reduced
28     O3 treatment to establish a potential adverse effect.
29          The 1986 (U.S. Environmental Protection Agency, 1986) made the following statement:
30     "The characterization and representation of plant exposures to O3 has been and continues to
       December 1993                          5.151      DRAFT-DO NOT QUOTE OR CITE

-------
 1     be a major problem because research has not yet clearly identified which components of the
 2     pollutant exposure cause plant response". This is still true today (See Section 5.5).
 3          The aim of most air pollution research experiments have been designed to quantify the
 4     relationship between pollutant exposure an agricultural crop yield.  The problem is the
 5     incorporation of the concentration, duration, frequency, age,  genetic composition and respite
 6     time into an exposure statistic or index which may be used to predict yield loss.  The correct
 7     exposure representation is the amount of pollutant entering the plant, not the ambient
 8     concentration to which it is exposed (Taylor et al.,  1982a;  Tingey  and Taylor, 1982).  Most
 9     indices were  not developed from a biological basis, nor were they  developed using an
10     experimental  approach specifically designed to address all key factors (Lee et al., 1990).
11     A number or exposure indices have been developed in an attempt for depicting plant response
12     to O3 exposure (See Section 5.5).  Much of the data in this section is evaluated using these
13     indices.  For this reason  several different exposure  statistics are used to determine the effect
14     of an exposure on plant response.  It should be remembered that the SUM06, which is used
15     more than any of the other indices, is the seasonal  sum of hourly concentrations at or above
16     0.06 ppm (See Section 5.5).
17           Exposure indices calculated  for each  of 10 years (1982  to 1991) and two exposure
18     periods,  June through August (three month) and May through September (five month) are
19     presented in Table 5-17 (modified from Tingey, et  al., 1991).  The monitoring data,
20     collected at non-urban sites, show that ambient O3  is frequently at, or near, the 7 h seasonal
21     mean (M7) that would be expected to cause a yield loss in crops based on the conclusions of
22     the 1986 criteria document.  This table may be used for comparison of ambient-O3
23     concentrations to those used in experiments.   Thirty-five percent of the 38 species or
24     cultivars under consideration would be predicted to have a 10% yield loss at a 7 h mean
25     concentration of between 0.04 and 0.05 ppm, but only 19%  required a 7 h mean
26     concentration of greater than 0.08 ppm to suffer a  predicted  10%  loss in yield.  Furthermore,
27      11 % of  the 38 species or cultivars would be expected to have a yield reduction of 10% at a
28      7 h mean or less than 0.028 to 0.035 ppm (Table 6-17, U.S. Environmental Protection
29      Agency, 1986).  It was also concluded that grain crops (with the exception of a few very
30      sensitive cultivars) were generally less sensitive than others,  but that within-species
31      variability in sensitivity may be as great or greater than between species. These results are

        December 1993                          5-162       DRAFT-DO NOT QUOTE OR CITE

-------
 TABLE 5-17. SUMMARY OF OZONE EXPOSURE INDICES CALCULA1
            3- OR 5-MONTH GROWING SEASONS FROM 1982 TO 1991
                                       FOR
3 mo
Year
1982
1983
1984
1985
1986
1987
1988
1989
1990
1991
(June-August)
HDM2
No. ppm
Sites
99
102
104
117
123
121
139
171
188
199
Among Years
5 mo
Mean CV
0.114 23
0.125 24
0.117 24
0.117 24
0.115 21
0.119 22
0.129 21
0.105 23
0.105 21
0.106 22
0.113 11
.7%
.9%
.6%
.6%
.8%
.9%
.3%
.1%
.6%
.0%
.1%
M7
ppm
Mean
0.052
0.056
0.052
0.052
0.052
0.055
0.060
0.051
0.053
CV
18.7%
21.9%
18.2%
17.1%
19.1%
17.6%
17.8%
17.5%
18.3%
0.054 18.4%
0.054 10.0%
SUMOO
ppnrh
Mean
82.9
86.1
84.1
84.6
85.3
86.9
97.6
86.4
85.7
87.7
87.0
CV
19.1%
22.1%
19.9%
18.0%
18.0%
17.3%
19.6%
19.9%
21.0%
21.3%
9.9%
SUM06
ppm-h
Mean
26.8
34.5
27.7
27.4
27.7
31.2
45.2
24.8
25.8
28.3
29.5
CV
68.8%
58.1%
58.4%
59.6%
65.0%
56.4%
46.8%
78.7%
76.2%
74.2%
42.1%
SIGMOID
ppm-h
Mean
26.3
33.0
27.4
27.4
27.7
30.4
42.9
25.8
26.6
28.9
29.4
CV
56.7%
52.3%
47.9%
47.6%
51.8%
46.8%
42.4%
59.4%
59.2%
59.5%
31.0%
(May-September)
M7

Year
1982
1983
1984
1985
1986
1987
1988
1989
1990
1991
No.
Sites
88
87
95
114
118
116
134
158
172
190
Among Years
ppm
Mean
0.048
0.051
0.048
0.048
0.048
0.050
0.054
0.047
0.049
0.050
0.049
SUMOO
ppm
CV Mean
20
22
18
18
20
20
18
18
19
19
9
.6%
.1%
.0%
.4%
.3%
.3%
.7%
.6%
.8%
.8%
.8%
122.9
129.6
126.2
124.5
123.3
128.7
141.7
127.8
129.4
130.6
129.0
•h
CV
22.3%
24.4%
19.1%
19.4%
21.4%
20.4%
22.0%
22.5%
22.7%
23.6%
9.9%
SUM06

ppm-h

SIGMOID
ppm-
Mean CV Mean
37.
44.
36.
36.
34.
3 70.
4 61.
7 60.
2 63.
9 70.
42.2 62.
58.
0 50.
32.7 87.
34.6 82.
36.8 80.
38.7 42.
9%
9%
8%
8%
7%
0%
5%
8%
7%
7%
5%
37.1
43.8
37.6
37.0
35.6
41.8
55.6
35.2
37.0
38.8
39.6
h
CV
57.8%
52.7%
46.9%
50.3%
55.7%
50.3%
45.0%
64.1%
62.1%
62.9%
29.8%
aUpdated and additional years from data given in Table HI of Tingey et al (1991) where the spatial and
 temporal variation in ambient O3 exposures is expressed in terms of several exposure indices.
 No. sites indicates the number of separate monitoring sites included in the analysis. Fewer sites had 5 mo of
 available data than 3 mo of available data.  The 2nd HDM index is calculated for sites with at least 3 mo of
 available data.
CSUMOO, SUM06, M7, SIGMOID, and 2nd HDM are the cumulative sum above 0.0 ppm, the cumulative sum
 above 0.06 ppm, the 7 h seasonal mean, the sigmoid weighted summed concentration, and the second highest
 daily maximum 1 h concentration, respectively.
 CV = coefficient of variation.

Source: Tingey et al. (1991).
December 1993
5-163
DRAFT-DO NOT QUOTE OR CITE

-------
 1     similar to those previously obtained from Table 6-19 in the 1986 document.  Lee et al.
 2     (1993a) have revised Table 6-19 (see Table 5-16) in U.S. Environmental Protection Agency
 3     (1986) using re-calculated peak-weighted exposure indices (shown to be more appropriate
 4     than long-term means for relating effects to ambient concentrations) for the 54 studies
 5     (Tables 5-18 and 5-19).
 6          In 1992, a Supplement to the Air Quality Criteria Document for Oxidants reviewed
 7     effects of oxidant exposure on vegetation.  Considerable emphasis was placed on the
 8     appropriate exposure index for relating biological effects of O3 on plants (U.S.
 9     Environmental Protection Agency, 1992).  An analysis of the data at that time showed that a
10     seasonal mean concentration (e.g., 7 or 24-h) might not be the best  expression of the
11     exposure since it did not weight high concentrations differently from low concentrations and
12     it did not account for the variable length of growing seasons or exposure durations.
13     Unfortunately, it is often impossible to calculate the different possible exposure indices
14     (means,  cumulative peak-or threshold-weighted, or continuously weighted [sigmoid]
15     cumulative) from information given in published papers.  Thus, difficulties remain in
16     comparing exposure-response studies that utilize different exposure indices.  However,
17     reported responses and concentrations  of O3 can be compared to those that occur at ambient
18     concentrations, and thence to other exposure indices (Table 5-17).
19
20     5.6.3.1   Effects of Ozone on Short-Lived (Less  Than 1-Year) Species
21           Plant species can be characterized by their life-span, either short-lived  annual species,
22     or longer-lived perennials and trees.  Physiological processes may be  related to life-span (for
23     instance, leaf gas exchange tends to be lower in longer-lived trees than in crop species) and
24     so, the response to O3 may be different  (Reich, 1987).  In addition, multiple year exposures
25     and carry-over effects  may be of importance in long-lived species, but of no concern in
26     annuals.  Accordingly, animals and perennials will be discussed  separately.  The response of
27     plants to O3 is also affected by interactions with other physical, chemical, and biological
28     factors.  Those interactions are discussed elsewhere in this document  (Section 5.3).  In most
29     cases, the research analyzed here was conducted under near-optimal conditions of water and
30     nutrient availability. While deviations from these conditions may affect the  magnitude of
        December 1993                          5-164      DRAFT-DO NOT QUOTE OR CITE

-------
TABLE 5-18. COMPARISON OF EXPOSURE-RESPONSE CURVES CALCULATED
   USING THE 3-MONTH, 24-HOUR SUM06 VALUES FOR 54 NCLAN CASES
Species
Barley (Linear)
Barley (Linear)
Corn(L)
Corn (L)
Cotton (L)
Cotton (L)
Cotton (L)
Cotton (L)
Cotton (L, Linear)
Cotton (L, Linear)
Cotton
Cotton
Cotton
Kidney Bean
Kidney Bean (L)
Lettuce (T)
Peanut (L)
Potato
Potato
Sorghum
Soybean
Soybean
Weibull/Linear Model
Parameters
Cultivar Moisture* ABC
CM-72 DRY
CM-72 WET
PIO
PAG
ACALA DRY
ACALA WET
ACALA DRY
ACALA WET
ACALA DRY
ACALA WET
STONEVILLE
MCNAIR DRY
MCNAIR WET
CAL LT RED
CAL LT RED
EMPIRE
NC-6
NORCfflP
NORCfflP
DEKALB
CORSOY
CORSOY
7741.1
8776.6
9627.4
10730.1
6465.0
9808.0
7009.8
7858.8
5.693
5.883
3576.1
3698.8
4811.0
2488.2
2484.3
7196.6
6402.5
5900.7
5755.6
8046.2
2652.6
1891.7
-4.412
15.485
92.61
94.36
92.59
71.17
83.78
78.01
-0.0011
-0.0017
94.6
165.81
117.02
27.41
44.24
54.87
100.12
93.84
79.26
178.05
57.1
65.21
2.823
4.316
2.361
1.997
1.849
1.311


2.012
2.778
1.534
3.885
2.691
5.512
2.226
1.000
1.654
2.338
1.726
5.160
RMSE°
1215
1175
680
1248
1097
521
949
937
104
90
226
342
366
333
397
613
351
742
675
441
166
282
3 mo 24-h
SUM06e
Values for Yield
Losses of
R2 10% 30%
0.12
NA
0.93
0.80
0.45
0.96
0.80
0.85
0.06
0.20
0.91
0.46
0.89
0.72
0.71
0.74
0.97
0.63
0.49
0.48
0.91
0.63
175.5
250.0
41.7
56.0
35.7
23.1
24.8
14.0
94.9
60.3
30.9
73.8
27.0
15.4
19.2
36.5
36.4
9.9
20.3
68.0
15.5
42.2
526.4
250.0
64.3
74.3
59.8
42.5
48.0
35.5
321.3
204.0
56.7
114.4
59.7
21.0
30.2
45.5
63.0
33.5
42.5
114.6
31.4
53.4
December 1993
5-165
DRAFT-DO NOT QUOTE OR CITE

-------
      TA&LE 5-18 (cont'd).  COMPARISON OF EXPOSURE-RESPONSE
  CURVES CALCULATED USING THE 3-MONTH, 24-HOUR SUM06 VALUES
                     FOR 54 NCLAN CASES
Species
Soybean
Soybean
Soybean
Soybean
Soybean
Soybean
Soybean
Soybean
Soybean
Soybean
Soybean
Soybean
Soybean
Soybean
Soybean
Soybean
Soybean
Soybean
Soybean
Soybean
Tobacco (L)
Turnip (T)
Turnip (T)
Turnip (T)
Cultivar
AMSOY
PELLA
WILLIAMS
CORSOY
CORSOY
CORSOY
CORSOY
CORSOY
CORSOY
WILLIAMS
WILLIAMS
HODGSON
DAVIS
DAVIS
DAVIS
DAVIS
DAVIS
DAVIS
YOUNG
YOUNG
MCNAIR
JUST RIGHT
PURPLE TOP
SHOGOIN
Weibull/Linear Model
Parameters
Moisture* ABC



DRY
WET
DRY
WET
DRY
WET
DRY
WET



DRY
WET
DRY
WET
DRY
WET




1907.2
2619.9
2368.4
2229.8
2913.8
3528.1
4905.0
5676.1
5873.9
6305.2
7338.4
2052.4
3929.7
4815.5
2007.1
4568.0
5775.6
8082.7
5978.8
7045.0
5177.4
12.7
5.7
4.4
75.
174.
146.
92.
311.
91
13
37
0
04
103.83
117.98
97.46
65.73
99.18
78.71
79.97
131.57
85.71
542.36
158.57
90
113
183
145
172
25
29
29
.18
.89
.63
.63
.55
.68
.26
.18
2.739
1.000
1.000
9.593
1.527
15.709
3
1
1
1
1
1
1
1
1
1
3
1
1
1
1
1
.590
.000
.319
.456
.344
.000
.000
.734
.000
.539
.348
.442
.448
.277
.186
.806
1.437
1
.548
RMSEC
390
311
527
193
330
400
401
508
512
389
377
361
524
346
556
495
920
927
244
424
306
0.810
0.590
0.660
,d
R2
0.41
0.51
0.27
0.16
0.38
0.55
0.80
0.81
0.89
0.87
0.94
0.78
0.64
0.87
0.04
0.61
0.55
0.71
0.93
0.93
0.81
0.96
0.92
0.81
3 mo 24-h
SUM066
Values for Yield
Losses of
10% 30%
33.4
18.3
15.4
72.8
71.3
90.0
63.0
10.3
11.9
21.1
14.8
8.4
13.9
23.4
57.1
36.8
46.0
23.9
38.8
25.0
25.9
7.4
6.1
6.8
52.1
62.1
52.2
82.6
158.4
97.2
88.5
34.8
30.1
48.8
36.5
28.5
46.9
47.3
193.4
81.2
66.3
55.7
90.1
65.0
72.3
14.5
14.3
15.0
December 1993
5-166
DRAFT-DO NOT QUOTE OR CITE

-------
                TABLE 5-18 (cont'd).  COMPARISON OF EXPOSURE-RESPONSE
          CURVES CALCULATED USING THE 3-MONTH, 24-HOUR SUM06 VALUES
                                      FOR 54 NCLAN CASES
3 mo 24-h
SUM06e
Weibull/Linear Model
Parameters
Species
Turnip (T)
Wheat
Wheat
Wheat
Wheat
Wheat
Wheat
Wheat
Cultivar
TOKYO
CROSS
ABE
ARTHUR
ROLAND
ABE
ARTHUR
VONA
VONA
Moisture* A
11.7
5149.8
4455.8
5028.9
6043.1
5446.9
5384.0
4451.0
B
27.83
52.89
60.87
52.32
47.39
72.34
27.74
33.5
C
2.142
3.077
2.176
1.173
7.711
2.462
1.000
1.818
RMSE6
3.250
399
264
405
226
349
608
654
2d
R2
0.78
0.90
0.92
0.91
0.74
0.57
0.88
0.64
Values for Yield
Losses of
10%
9.7
25.5
21.6
7.7
35.4
29.0
2.9
9.7
30%
17.2(
37.8
37.9
21.7
41.5
47.6
9.9
19.0
      aWet refers to experiments conducted under well-watered conditions while dry refers to experiment conducted
       under some controlled level of drought stress.
      bFor those studies whose species name is followed by "(Linear)" a linear model was fit.
       A Weibull model was fit to all other studies and estimates of B parameter are in ppm-h.  The
       yield is expressed in kg/Ha for all crops except turnip (g/plant) and lettuce (g/m).  In cases
       where the estimated C parameter is exactly 1.0, the shape parameter has been bounded from
       below to obtain convergence in the nonlinear model fitting routine. For those studies whose
       species name is followed by "(L)" a log transformation was used to stabilize the variance. For
       those crops whose name is followed by "(T)" the yield is expressed as either g/plant or g/m.
      cThe root mean square error based on individual plot means.
      dR2 or multiple correlation coefficient measures the proportion of total variation about the mean
       response explained by the regression on individual plot means..
      eThe 24-h SUM06 value (ppm-h) that was predicted to cause a 10 or 30% yield loss
       (compared to zero SUM06).

      Source:  Lee et al. (1993b).
1      response, it is important to understand the potential of Oj exposure, and to understand the
2      consequences.
3           Several papers (Lee et al.,  1988, 1991, 1993a,b; Lefohn et al., 1988; Lesser et al.,
4      1990; Tingey et al., 1991) present a re-analysis of NCLAN data and/or data from field
       December 1993
5-167       DRAFT-DO NOT QUOTE OR CITE

-------
TABLE 5-19. COMPARISON OF EXPOSURE-RESPONSE CURVES CALCULATED
       USING THE 24-HOUR W126 VALUES FOR 54 NCLAN CASES
Species
Cultivar Moisture* A
Barley
Barley
Corn (L)
Corn (L)
Cotton
Cotton
Cotton
Cotton
Cotton
Cotton
Cotton
Cotton
Cotton
(L)
(L)
(L)
(L)
(L)
(L)



Kidney Bean
Kidney Bean (L)
Lettuce (T)
Peanut
Potato
Potato
(L)


Sorghum
Soybean
Soybean
CM-72 DRY
CM-72 WET
PIO
PAG
ACALA DRY
ACALA WET
ACALA DRY
ACALA WET
ACALA DRY
ACALA WET
STONEVILLE
MCNAIR DRY
MCNAIR WET
CALLTRED
CAL LT RED
EMPIRE
NC-6
NORCfflP
NORCfflP
DEKALB
CORSOY
CORSOY
Weibullb
B
8133.2 1109.6
8927.2 57439.6
9605.0 92.9
10686.7 94.5
6482.8
9817.
7022.
7927.
310.
393.
3
7
1
1
2
3592.1
3700.9
4817.6
2484.7
2475.2
7197.4
6386.0
5867
.2
5777.9
8049.7
2660
1895
.3
.6
89.9
66.6
81.3
74.7
174.1
582.6
94.1
174.1
113.5
28.0
44.2
54.6
97.4
96.3
113.9
205.9
58.8
63.3
C RMSEC
1.000 1214
1.000 1175
2.594 650
4.1901253
1.949 1075
1.603
1.540
1.070
2.189
1.000
1.582
2.430
1.410
3.706
2.353
4.921
1.905
1.000
1.299
1.963
1.455
4.032
514
948
943
104
90
223
344
360
332
401
614
370
754
675
439
169
280
2d
R2
0.13
NA
0.93
0.80
0.47
0.96
0.80
0.85
0.06
0.20
0.91
0.45
0.89
0.72
0.70
0.74
0.96
0.62
0.48
0.48
0.91
0.63
24-h W126e
Values for Yield
Losses of
10% 30%
116.
6051.
39.
55.
28.
16.
18.
9.
62.
61.
22,
68.
23.
15.
17
34
9 395.8
9 20487.3
0 62.4
2 73.9
3
4
8
1
,3
,4
,7
9
.0
.3
.0
.6
29.9
10
20
65
12
36
.1
.1
.4
.5
.2
53.0
35.0
41.6
28.5
108.7
207.8
49.1
113.9
54.6
21.2
28.5
44.3
56.7
34.3
51.5
121.8
28.9
49.0
December 1993
5-168    DRAFT-DO NOT QUOTE OR CITE

-------
   TABLE 5-19 (cont'd). COMPARISON OF EXPOSURE-RESPONSE CURVES
  CALCULATED USING THE 24-HOUR W126 VALUES FOR 54 NCLAN CASES
Species
Soybean
Soybean
Soybean
Soybean
Soybean
Soybean
Soybean
Soybean
Soybean
Soybean
Soybean
Soybean
Soybean
Soybean
Soybean
Soybean
Soybean
Soybean
Soybean
Soybean
Cultivar
AMSOY
PELLA
WILLIAMS
CORSOY
CORSOY
CORSOY
CORSOY
CORSOY
CORSOY
WILLIAMS
WILLIAMS
HODGSON
DAVIS
DAVIS
DAVIS
DAVIS
DAVIS
DAVIS
YOUNG
YOUNG
Moisture A
Weibullb
B
1926.1
2602.4
2341.8
DRY
WET
DRY
WET
DRY
WET
DRY
WET

2229.3
2929.7
3533.5
4909.5
5597.1
5884.8
6314
7352
2044
.1
.3
.6
3837.6

DRY
WET
DRY
WET
DRY
WET
4810
1992
4595
.8
.3
.4
5770.1
8101
.3
5994.2
7075.0
79.0
161.
138.
88.
5
6
2
470.2
113.
126.
2
5
95.7
65.6
106.3
80.7
76.2
130.3
87.5
537.6
170.9
90.6
118
199
.2
.8
149.7
C RMSEC
1.977
1.000
1.000
8.632
1.128
11.095
2.803
1.000
1.139
1.243
1.162
1.000
1.000
1.494
1.000
1.253
2.796
1.220
1.251
1.133
390
314
533
192
329
403
405
526
515
391
368
361
530
352
558
496
928
939
244
418
R2
0.41
0.50
0.25
0.16
0.39
0.54
0.80
0.80
0.88
0.87
0.95
0.78
0.63
0.86
0.03
0.61
0.54
0.70
0.93
0.93
24-h W126e
Values for Yield
Losses of
10% 30%
25.3
17.0
14.6
67.9
64.0
92.4
56.7
10.1
9.1
17.4
11.6
8.0
13.7
19.4
56.6
28.4
40.5
18.7
33.1
20.5
46.9
57.6
49.4
78.2
188.6
103.1
87.6
34.1
26.6
46.4
33.2
27.2
46.5
43.9
191.7
75.1
62.7
50.8
87.7
60.2
December 1993
5-169    DRAFT-DO NOT QUOTE OR CITE

-------
    TABLE 5-19 (cont'd).  COMPARISON OF EXPOSURE-RESPONSE CURVES
   CALCULATED USING THE 24-HOUR W126 VALUES FOR 54 NCLAN CASES
Species
Tobacco (L)
Turnip (T)
Turnip (T)
Turnip (T)
Turnip (T)
Wheat
Wheat
Wheat
Wheat
Wheat
Wheat
Wheat
Weibullb
Cultivar Moisture* A B
MCNAIR
JUST RIGHT
PURPLE TOP
SHOGON
TOKYO
CROSS
ABE
ARTHUR
ROL
ABE
ARTHUR
VONA
VONA
5223.9
12.7
5.8
4.4
11.7
5138.1
4467.4
5074.4
6042.8
5440.0
5300.8
4462.7
179.8
24.1
28.2
28.2
26.8
53.3
63.8
51.2
48.5
76.1
25.0
32.3
C RMSEC
1.018 291
1.473 0.96
1.155 1
1.174 1
1.710 3
2.602 407
1.747 264
1.000 397
5.843 225
2.100 349
1.000 679
1.517 665
2d
R2
0.83
0.92
0.82
0.78
0.89
0.92
0.91
0.75
0.57
0.85
0.63
24-h W126e
Values for Yield
Losses of
10% 30%
19.7
5.21
4.0
4.1
7.2
22.4
17.6
5.4
33.0
26.1
2.6
7.3
65.3
2.0
11.6
11.7
14.7
35.8
35.4
18.3
40.6
46.6
8.9
16.4
 Wet refers to experiments conducted under wll-watered conditions while dry refers to experiments conducted
 under some controlled level of drought.
 All estimates of B parameter are in ppm-h. The yield is expressed in kg/Ha for all crops except turnip
 (g/plant) and lettuce (g/m). In cases where the estimated C parameter is exactly 1.0, the shape parameter has
 been bounded from below to obtain convergence in the nonlinear model fitting routine.  For those studies
 whose species name is followed by "(L)" a log transformation was used to stabilize the variance. For those
 crops whose name is followed by "(T)" the yield is expressed as either g/plant or g/m.
cThe root mean square error based on individual plot means.
 R  or multiple correlation coefficient measures the proportion of total variation about the mean response
 explained by the regression on individual plot means.
"The 24-h W126 value (ppm-h) that was predicted to cause a 10 or 30% yield loss (compared to zero
 W126).

Source: Lee et al. (1993b).
December 1993
5-170      DRAFT-DO NOT QUOTE OR CITE

-------
 1     studies conducted on potato that were not part of the NCLAN project. Lee et al. (1988,
 2     1991) examined a number of measures of O3 exposure in relation to response data collected
 3     in the experiments.  They were particularly interested in examining the ability of a seasonal
 4     mean,  a cumulative exposure  index, and the second highest daily maximum concentration
 5     (2HDM) to predict  the biological response of the plant. They found that no particular index
 6     of O3 concentration dominated as best in all studies, but that cumulative indexes that
 7     weighted high concentrations at the "grain-filling"  stage of the life cycle were better than a
 8     seasonal mean.  Seasonal means did work well within a given experiment where treatments
 9     were highly correlated.  The 2HDM was consistently a poor predictor of plant response.
10          In a re-analysis of NCLAN data, Lesser et al. (1990) presented composite exposure-
11     response functions for a number of crop species, or groups of species.  Predicted yield losses
12     (compared to yield  at an assumed background concentration of 0.025 ppm) of up to 20%
13     occurred at a 12 h  seasonal  mean of 0.06 ppm, with a loss of 10% at a 12 h mean
14     concentration of about 0.045 ppm.
15          Tingey et  al.  (1991) and Lee et al. (1993) went on to re-analyze the crop response data
16     using three measures of exposure:   (1) the SUM06 (the cumulative sum of all hourly
17     O3 concentrations greater than 0.06 ppm), (2) the  7 h seasonal mean, and (3) the 2HDM.
18     Their analysis included crops  that account for 70% of all crop land in the United States and
19     73% of the agricultural receipts.  The analysis included 31 field experiments with 12 crop
20     species, conducted  in open-top chambers and resulted in composite exposure-response
21     functions.  The results of their studies and additional re-analyses done since then are
22     summarized in Tables 5-20  and 5-21.  They concluded that to limit yield loss to 10% or less
23     in 50% of the cases (all experiments and crops), a SUM06 of 24.4 ppnvh (or 26.4 ppm-h
24     based on 24 h), a 7 h seasonal mean of 0.049 ppm, or a 2HDM of 0.094 ppm would be
25     required.  A SUM06 of about 37 ppnvh should limit yield losses to 20%  in 50% of the
26     cases.  If one standard error were added to or subtracted account for the variability, the
27     metrics would be reduced to 21, 0.046, and 0.088 or increased to 27.8 ppm-h, 0.049 ppm
28     and 0.10 ppm respectively.  To limit the loss to 10% or less in 75% of the cases would
29     require 14.2 ppm-h, 0.040 ppm and 0.051 ppm respectively (Table 5-20).  These values are
30     based on studies of both well-watered and drought stressed plants.
       December 1993                          5.171      DRAFT-DO NOT QUOTE OR CITE

-------
             TABLE 5-20.  THE EXPOSURE LEVELS (USING VARIOUS INDICES)
                  ESTIMATED TO CAUSE AT LEAST 10% CROP LOSS IN
                          50 AND 75% OF EXPERIMENTAL CASES
50th Percentile No.
NCLANData(N=49;
NCLAN Data (N=39;
NCLAN Data (N=54;
NCLAN Data (N = 42;
NCLAN Data (N= 10;
NCLAN Data (N= 10;
Cotton Data (N=5)
Soybean Data (N=13)
Wheat Data(N=6)
Cotton Data(N=5) **
Soybean Data (N= 15)
Wheat Data (N=7) **
75th PERCENTILE #
NCLAN Data (N = 49;
NCLAN Data (N= 39;
NCLAN Data (N =54;
NCLAN Data (N = 42;
NCLAN Data (N= 10;
NCLAN Data (N= 10;
Cotton Data (N=5)
Soybean Data (N = 13)
Wheat Data (N=6)
Cotton Data (N=5) **
Soybean Data (N=15)
Wheat Data(N = 7) **
SUM06
Wet and Dry) (?)
Wet Only)
Wet and Dry) **
Wet Only) **
Wet)
Dry)




**


Wet and Dry)
Wet Only)
Wet and Dry) **
Wet Only) **
Wet)
Dry)




**

24.4
22.3
26.4
23.4
25.9
45.7
23.6
26.2
21.3
30.0
23.9
25.9

14.2
14.3
16.5
17.2
16.4
24.0
21.8
14.2
11.7
21.1
15.3
5.1
SE* S1GMOID
3.
1.
3.
3.
4.
23.
4
0
2
1
5
3
2.3
5.
4
15.2
12.7
6.5
10.5

4,
2,
4
3
3
0
5
0
2
6
4
2

.2
.7
.3
.0
.7
.8
.0
.1
.5
.0
.1
.6
21.
19.
23.
22.
23.
40.
19.
22.
5
4
5
9
4
6
3
6
19.3
27.2
22.0
21.4


11.9
12.6
14.5
14.7
13
22
17
12
10
16
13
8
.7
.3
.5
.4
.9
.7
.4
.5
SE
2.0
2.3
2.4
4.7
3.2
0.1
2.3
3.6
12.7
12.8
8.0
9.4

5.6
2.3
3.2
2.4
3.2
0.1
2.8
0.1
2.4
5.7
4.1
3.4
M7
0.049
0.046
NA
NA
0.041
0.059
0.041
0.044
0.061
NA
NA
NA

0.040
0.039
NA
NA
0.040
0.053
0.041
0.041
0.054
NA
NA
NA
SE 2ndHDM
0.003
0.003
NA
NA
0.001
0.014
0.001
0,005
0.018
NA
NA
NA

0.007
0.005
NA
NA
0.001
0.022
0.001
0.006
0.032
NA
NA
NA
0.094
0.090
0.099
0.089
0.110
0.119
0.066
0.085
0.098
0.075
0.088
0.097

0.051
0.056
0.073
0.070
0.080
0.093
0.065
0.069
0.062
0.070
0.078
0.054
SE
0.006
0.010
0.011
0.008
0.042
0.017
0.032
0.013
0.059
0.012
0.008
0.028

0.010
0.006
0.006
0.006
0.032
0.003
0.014
0.004
0.035
0.034
0.007
0.027
      # The numbers in parentheses are the number of cases used in deriving the various exposure levels.
      * Standard error (SE).
      ? NCLAN data refers to studies conducted as part of the NCLAN project. Wet and dry refer to watery regimes
       used in the studies, wet being well-watered, and dry meaning some level of drought stress was imposed.
      ** 24-h exposure statistics reported in Lee et al. (1993). Relative yield loss for 2ndHDM is relative to yield at
        0.04 ppm rather than 0.00 ppm as was used in Tingey et al. (1991).

      Modified from:  Tingey et al. (1991).
1          A further analysis by Lee et al. (1993b) provides composite exposure-response
2     functions for all NCLAN studies, as well as for soybean and wheat experiments
3     (Table 5-21).  In the analysis, they calculated the SUM06 based on 24 h per day
      December 1993
5-172
DRAFT-DO NOT QUOTE OR CITE

-------
   TABLE 5-21. SUM06 LEVELS ASSOCIATED WITH 10 AND 20% YIELD LOSS
                  FOR 50 AND 75% OF THE NCLAN CROP STUDIES
Weibull equations (all 54 NCLAN studies):

50th Percentilea PRYL =  1 - exp(-[SUM06/89.497]**1.84461)
75th Percentile PRYL = 1 - exp(-[SUM06/60.901]**l.72020)

Weibull equations (all 22 NCLAN soybean studies; 15 well-watered, 7 water-stress):

50th Percentile PRYL = 1 - exp(-[SUM06/l 17.68]**!.46509)
75th Percentile PRYL = 1 - exp(-[SUM06/88.99]**1.47115)

Weibull equations (15 NCLAN well-watered soybean studies):

50th Percentile PRYL = 1 - exp(-[SUM06/l 12.75]**!.46150)
75th Percentile PRYL = 1 - exp(-[SUM06/79.62]** 1.36037)

Weibull equations (7 NCLAN wheat studies):

50th Percentile PRYL = 1 - exp(-[SUM06/49.02]**3.52788)
75th Percentile PRYL = 1 - exp(-[SUM06/29.56]**l .29923)

SUM06 levels associated with 10% and 20% yield loss for 50% and 75% of the crops.

All 54 NCLAN cases
                            Relative     10%
                            Yield Loss   20%
       Percent of crops
       50%    75%
       26.4    16.5
       39.7    25.5
All 22 NCLAN soybean cases
 15 well-watered soybean cases
All 7 NCLAN wheat cases
                             Relative
                             Yield Loss
                             Relative
                             Yield Loss
10%
20%
10%
20%
                             Relative
                             Yield Loss   20%
Percent of crops
50%    75%
25.3    19.3
42.3    32.1
Percent of crops
50%   75%
24.2   15.2
40.4   26.4
       Percent of crops
       50%   75%
       25.9   5.2
       32.0   9.3
 50th and 75th percentile refer to the percentage of studies analyzed in which loss of the stated magnitude would
 have been prevented.

Source:  Lee et al. (1993a,b).
December 1993
   5-173
        DRAFT-DO NOT QUOTE OR CITE

-------
 1      03 concentrations and the  resulting exposure to prevent crops from yield loss is slightly
 2      higher than they previously calculated (26.4 ppnvh versus 24.4 ppnvh, Table 5-20).
 3      A composite exposure-response function based on uncited data using GIS, TRIGRO and
 4      ZELIG models is illustrated in Figure 5-22.
 5           Research since 1986  has largely focused on understanding the response of trees and
 6      other perennials to O3 (covered in the next section) and of five crop species: cotton, wheat,
 7      spring rape, Phaseolus bean, and soybean.  A number of the studies were conducted as part
 8      of NCLAN, but many were also the result of research activity in Europe.  Results  of these
 9      studies,  as well as those species studied less intensively,  are summarized in Table 5-22.
10           Yield losses in cotton of 13 to 19%  have been reported at 12 h mean concentrations of
11      0.050 or 0.044 ppm by Heagle et al. (1988), Miller et al. (1988), and Temple  et al. (1988b)
12      (Table 5-22).  These are typical ambient concentrations as listed under M7 (Table 5-17).
13      The same experiments showed that drought stress reduced the predicted yield loss due to O3,
14     but did not eliminate it.
15          Wheat yields have been reduced by  0 to 29%, depending on the cultivar  and  exposure
16     conditions (Adaros et al.,  1991a; Fuhrer et al.,  1989; Grandjean and Fuhrer, 1989; Kohut
17     et al., 1987; Pleijel et al.,  1991) (Table 5-22).   In no case was a 7 h average of greater than
18     0.062 ppm required to cause the reported loss, but Slaughter et al. (1989) suggest that hourly
19     concentrations above 0.06 ppm during the period following  anthesis may be particularly
20     effective in reducing yield.
21           Studies with spring rape in Europe have documented yield losses of 9.5 to 26.9% at
22     8 h growing season average concentrations ranging from 0.03 to 0.06 ppm (Adaros et al.,
23      1991b,c) (Table 5-22).
24           The yield of Phaseolus beans (fresh pods) was reduced by 17% at a 7 h  average of
25     0.045 ppm (Schenone et al., 1992) or 20% at an 8 h growing season average  of 0.080 ppm
26      (Bender et al., 1990). In a similar study, Heck et al. (1988) the predicted yield of sensitive
27      cultivars was  reduced an average of 17.3% by exposure to  a 7 h growing season mean of
 28      0.05 ppm, but resistant cultivars suffered only a 1.6% loss.  Temple (1991) reported
 29      reductions in  dry bean yield of 44 to 73% in three cultivars grown in California and exposed
 30     to a 12 h seasonal mean of 0.072  ppm.  One other cultivar increased in yield  hi non-filtered
        December 1993                          5-174      DRAFT-DO NOT QUOTE OR CITE

-------
                                                                 75th percontile
                                                                 50th peroentite
                                                                 25th percentfte
                  ~r
                  10
       "i
       20
            100%-]

             90%

             80%

             70%-:

           8 60%^

          S 50%-;

           £    '•
          •M 40%-
          •s    :
          & 30%-

             20%-

             10%-

             0%
  B. Tree Seedlings
                                   30       40
                                 24-h Sum06 (ppm-h)
   T
   50
"1"
60
^s^^	«H«	^^ _ »•»•" _— _
~i      "T"    "i""     "r	r"
 10       20       30       40       50
       24-h Sum06 (ppm-h) (adjusted to 92 days)
               75th percentile


              ; 50th percentile


              ' 25th percentile
                                                             "\~"
                                                             60
Figure 5-22.  Box-plot distribution of biomass loss predictions from Weibull and linear
             exposure-response models that relate biomass and ozone exposure as
             characterized by the 24-h SUM06 statistic using data from (A) 31 crop
             studies from the National Crop Loss Assessment Network (NCLAN)
             program and (B) 26 tree seedling studies conducted at the Environmental
             Research Laboratory in Corvallis, Oregon; Smoky Mountain National
             Park, Tennessee; Michigan; Ohio; and Alabama.  Separate regressions
             were calculated for studies with multiple harvests  and/or cultivars
             resulting in a total of 54 individuals equations from the 31 NCLAN studies
             and 56 equations from the 26 seedling studies.  Each equation was used to
             calculate the predicted relative yield or biomass loss at 10, 20, 30, 40, 50,
             and 60 ppnrh and the distributions of the resulting losses plotted.  The
             solid line is the calculated Weibull fit at the 50th percentile.  From Hogsett
             et al. (1993).
December 1993
                    5-175
DRAFT-DO NOT QUOTE OR CITE

-------
O
o
1

1











1
ON


O
^
H
6
o
2j
9
0
C
H
O
n
TABLE 5-22. A SUMMARY OF STUDIES REPORTING THE EFFECTS OF OZONE
ON THE GROWTH, PRODUCTIVITY, OR YIELD OF ANNUAL PLANTS PUBLISHED SINCE
U.S. ENVIRONMENTAL PROTECTION AGENCY (1986)

Species
Soybean




Soybean

Soybean



Soybean

Soybean

Soybean

Soybean



Soybean





E/D/
PC/Ca Concentration15
C 18 or 24 ppb vs. 59 or
72 ppb, 9 h mean



C 23, 40, and 66 ppb 7 h
mean
C 97 ppb vs. 38, 23, 16,
23 ppb 7 h mean


C 17 to 122 ppb 7 h mean

C 25 and 50 ppb 7 h mean

C 20 and 50 ppb 12 h mean

C 25 and 55 ppb 7 h mean



C 27 and 54 ppb 7 h means






Duration
13 weeks,
2 growing
seasons


84 days

4 31 day
periods,
1 growing
season
69 days

about 90 days

107 days

64, 70, and 62
days,
3 growing
seasons
about 109 and
103 days,
2 growing
seasons



Facility0 Variable41 Effect6
OTC seed yield 12.5% reduction over
filtered air averaged over
cultivars. Between caltivar
differences as great as ozone
effect.
OTC seed yield 15.8 and 29% reduction
over 23 ppb.
OTC seed yield 30 to 56 % reduction over
in pots control, most loss in mid to
late growth stage.

OTC seed yield 8% at 35 ppb to 41 % at 122
ppb.
OTC seed yield Predicted loss of 10%.

OTC seed yield Predicted loss of 13%.

OTC seed yield Predicted loss of 15%.



OTC seed yield Predicted loss of 12 and
14%.





Reference
Mulchi et al.
(1988)



Mulchi et al.
(1992)
Heagle et al.
(1991)


Kohut et al.
(1986)
Heagle et al.
(1986b)
Miller et al.
(1989)
Heggestad and
Lesser (1990)


Heagle et al,
(1987)





-------
TABLE 5-22 (cont'd). A SUMMARY OF STUDIES REPORTING THE EFFECTS OF
CD
1
J2 Species
Soybean

Soybean
Soybean
± Cotton
-j
U Cotton
fr
O Cotton
§
^? Cotton
§
H Cotton
o
i
o
UZAJrNJk UIN lilt LrKUWlH, itCULIUU 11V11 Y , UK YLfcLJJ Uf AN IN U AT, fJUAINlS
PUBLISHED SINCE U.S. ENVIRONMENTAL PROTECTION AGENCY (1986)
E/D/
PC/Ca Concentration6 Duration
C filtered and non-filtered about
air-concentration not 125 days
reported 2 growing
seasons
C 10 to 130 ppb 8 weeks,
6.8 h/day
C 200 ppb 12 h, up to
4 times
C 15 to 111 ppb 12 h mean 123 days
C 10 to 90 ppb 12 h mean 102 days

C 25 to 74 ppb 12 h mean 123 days
C 22 to 44 ppb 12 h mean 124 days
C 26 to 104 ppb 7 h mean 1 19 days


c d
Facility Variable
OTC seed yield

GC biomass
GC shoot and
root
weight
OTC leaf,
stem, and
root
weight
OTC lint
weight

OTC lint
weight
OTC lint
weight
OTC lint
weight


Effect6
No difference.

Predicted reduction of 16 or
33 % at 60 and 100 ppb vs
25 ppb.
No effect at maturity.
Up to 42 % reduction in leaf
and stem, and 6 1 %
reduction in root weights.
40 to 71 % reduction at
highest concentration
determinant cultivars more
susceptible.
Predicted loss of 26.2% at
74 ppb.
Predicted loss of 19% at
44 ppb.
Predicted loss of 1 1 % at
53 ppb.


Reference
Johnston and
Shriner (1986)

Amundson et al.
(1986)
Smith et al.
(1990)
Temple et al.
(1988c)
Temple (1990b)

Temple et al.
(1988b)
Heagle et al.
(1988)
Heagle et al.
(1986a)



-------
TABLE 5-22 (cont'd). A SUMMARY OF STUDIES REPORTING THE EFFECTS OF
1
^_ n
^O










i
!!j
oo


O

3
O
O
g
3
 10% in 8 lines at
63 ppb 7 h mearl.
15.5% reduction at 45 ppb
(3S» ppnvh).
3.5 to 26% reduction in
resistant and sensitive
cultivars at 55-60 ppb.

20% reduction at 80 ppb.




55 to 75 % reduction at
72 ppb 12 h mean,
198 highest hour.
26-42% reduction at 38 to
50 ppb.
growth response detected if
exposure separated by 3 to
5 days.
13% reduction at 40 ppb.






Reference
Eason and
Reinert (1991)

Schenone et al.
(1992)
Heck et al.
(1988)


Bender et al.
(1990)



Temple (1991)


Sanders et al.
(1992)
McCool et al.
(1988)

Fuhrer et al.
(1989)





-------
TABLE 5-22 (cont'd). A SUMMARY OF STUDIES REPORTING THE EFFECTS OF
OZONE ON THE GROWTH, PRODUCTIVITY, OR YIELD OF ANNUAL PLANTS
1
OJ



1
^3

o
1
o
1
o
§
o

Species
Wheat-Spring

Wheat-Spring

Wheat-Spring

Wheat-Spring

Wheat-Spring

Wheat-Spring
Wheat-Spring
Wheat-Spring
PUBLISHED SINCE U.S.
E/D/
PC/Ca Concentration0
C 21.6 to 80 and 24.6 to
93.5 ppm-h

C 3 to 56 ppb 7 h mean

C 8 to 101 and 20-221 ppb
8 h mean

C 0 to 38 ppb 8 h mean

C 17 to 77 ppb 7 h mean

C 25 to 75 ppb 8 h mean
C 6 to 10 ppb 6 h/day
C 10 to 125 ppb 6 h/day
ENVIRONMENTAL PROTECTION AGENCY (1986)
Duration
82 and
88 days in
2 growing
seasons
61 and
55 days in
2 growing
seasons
118 and
98 days in
2 growing
seasons
entire
growing
season
90 and
87 days hi
2 growing
seasons
40 days
21 days
21 days and
17 days
Facility0 Variable
OTC seed
weight

OTC seed
weight

OTC seed
weight

OTC seed
weight

OTC seed
weight

OTC total
weight
GC shoot dry
weight
GC top dry
weight
Effect6
48 to 54% reduction at
80 and 93.5 ppm-h.

7% reduction at 15 and
22 ppb.

10% reduction at 17 to
23 ppb.

5 % reduction at 38 ppb.

9.5 to 11.6 reduction at
37 and 45 ppb.

Reductions at 75 ppb.
Decreased 35-60% at
101 ppb in low and high
light.
Reduced by up to 35%.
Reference
Grandjean and
Fuhrer (1989)

Pleijel et al.
(1991)

Adaros et al.
(1991a)

DeTemmerman
et al. (1992)

Fuhrer et al.
(1992)

Johnsen et al.
(1992)
Mortensen
(1990b)
Mortensen
(1990c)

-------
December 1993








Y1
i


d
F
H
8
O
i
H
8
n
TABLE 5-22 (cont'd). A SUMMARY OF STUDIES REPORTING THE EFFECTS OF
OZONE ON THE GROWTH, PRODUCTIVITY, OR YIELD OF ANNUAL PLANTS
PUBLISHED SINCE U.S. ENVIRONMENTAL PROTECTION AGENCY (1986)
Species
Wheat-Winter

Wheat-Winter




Wheat-Winter


Wheat-Winter



Wheat-Winter

Barley-Spring
Barley-Spring
Barley-Spring



E/D/
PC/C* Concentration Duration
C 1 1 to 42 ppb 14 week 109 days
mean
C 30 to 93 ppb 4 h mean 39 and
40 days in
2 growing
5 day /week
4h/day
C 27 to 96 ppb 7 h mean 36 days


C 22 to 96 ppb 7 h mean 65 days and
36 days in
2 growing
seasons
C 23 to 123 ppb 4 h/day 5 days at
anthesis
C 6 to 45 ppb 7 h mean 96 days
C 0.6-27 ppb monthly mean growing
season
C 0.8-83 ppb 8 h mean 97, 108 and
98 days in
3 growing
seasons

Facility0
OTC

OTC




OTC


OTC



OTC

OTC
OTC
OTC in
pots


Variable*1 Effect6
seed No effect.
weight
seed Exposures > 60 ppb during
weight anthesis reduce yield.



seed 50% reduction at 96 ppb.
weight/
head
seed 33% and 22% reduction at
weight 42 and 54 ppb.


seed Up to 28% reduction.
weight
seed No effect.
weight
seed No effect.
weight
seed 0-13% reduction at highest.
weight


Reference
Olszyk et al.

Slaughter et al.
(1989)



Amundson et al.
(1987)

Kohut et al.
(1987)


Mulchi et al.
(1986)
Pleijel et al.
(1992)
Weigel et al.
(1987)
Adaros et al.
(1991b)



-------
TABLE 5-22 (cont'd). A SUMMARY OF STUDIES REPORTING THE EFFECTS OF
cr
u>










i
oo


o
§>
3
6
o
s
H
O
d
§

Species
Rape-Spring

Rape-Spring



Rape-Spring



Tomato

Tomato

Tomato

Silene acaulis

Plantago
lanceolata

16 other species

PUBLISHED SINCE U.S
E/D/
PC/CT Concentration
C 25 to 75 ppb 8 h mean

C 0.8-83 ppb 8 h mean



C 43 to 60 ppb 8 h mean



C 13 to 109 12 h mean
79.5 ppm h
C 10 to 85 ppb 6 h/day

C 18 to 66 ppb 12 h mean

5 to 80 ppb 8 h/day

5 to 80 ppb 8 h/day


5 to 80 ppb 8 h/day

••••"•J •m~ "m^r m-r ^s -^f -m. ,». • .M. -•. .«. • V^ A.^. .M. *.M^1M.*M,r x_*- .*. 4 ,•_*. 1 i ^ ^/ i » • -* JL M~*4. »' ^ i. fc_?
. ENVIRONMENTAL PROTECTION AGENCY (1986)
Duration
31 days

89, 113 and
84 days in
3 growing
seasons
89, 113 and
84 days in
3 growing
seasons
75 days

12-21 days

11 weeks

up to 90 days

up to 90 days


up to 90 days

Facility
OTC

OTCin
pots


OTCin
pots


OTC

GC

OTC

GC

GC


GC

Variable
premature
senescence
seed weight



seed weight



fresh
weight
shoot dry
weight
fresh fruit
weight
dry weight

dry weight


dry weight

Effect6
Increased at 75 ppb.

9.4-16% reduction at 30 or
51 ppb.


12-27% reduction.



17 to 54% reduction at 109,
no reduction at ambient.
35 to 62% reduction.

No effect.

25% reduction at 80 ppb.

14% reduction at 50 ppb.


No effect.

Reference
Johnsen et al.
(1992)
Adaros et al.
(1991b)


Adaros et al.
(1991c)


Temple (1990a)

Mortensen
(1992b)
Takemoto et al.
(1988c)
Mortensen and
Nilsen (1992)
Mortensen and
Nilsen (1992)

Mortensen and
Nilsen (1992)

-------
TABLE 5-22 (cont'd). A SUMMARY OF STUDIES REPORTING THE EFFECTS OF
a
B
O"
•i
MD









i
oo
NJ


o
£
i
§
5*
Q
H
O
c|
o
a
in

90
\JZjU in KJ UIN 1±1H, IjKUW 1
PUBLISHED SINCE U.S
Species
Radish

Lettuce

Lettuce

Faba bean

Fenugreek
Chickpea

Black-gram
Rice

Rice

Watermelon



Pea





E/D/
PC/Ca
C

c

c

c

c
c

c
c

c

c



c





Concentration
20 or 70 ppb 24 h mean

21 - 123 ppb 7 h mean

10 to 34 ppb 7 week
mean
6 or 15 ppb 24 h mean

120 ppb 7 h/day
120 ppb 7 h/day

120 ppb 7 h/day
0 to 200 ppb 5 h/day

50 ppb 24 h mean

15 to 27 ppb 7 h mean



10 to 35 ppb 12 h mean





±1, i-HUJLJLJ^HVH I, UK YlfcJLJJ U* AIN1NUA1-, JriiATVlS
. ENVIRONMENTAL PROTECTION AGENCY (1986)
Duration
27 days

52 days

64 days

134 days

4 weeks
4 weeks

4 weeks
5 days/week
15 weeks
8 weeks

81 days



58 and
52 days in
2 growing
seasons


Facility0
GC

OTC

OTC

ofc

CC
CC

CC
OTC

GC

OTC



OF





Variabled
shoot and
root growth
head weight

fresh weight

seed weight

dry weight
dry weight

dry weight
seed weight

dry weight

fresh weight
and number
(marketable)

fresh weight





Effect6
36 and 45% reduction al
70 ppb.
Significant reduction at
83 ppb, 35% at 128 ppb.
No effect.

No effect.

No significant effect.
No significant effect.

No significant effect.
12 to 21% reduction at
200 ppb.
No effect at 50 ppb.

20.8 and 21. 5%
reduction at 27 ppb.


linear decrease in yield
with increasing O3




Reference
Barnes and
Pfirrman (1992)
Temple et al.
(1986)
Olszyk et al.
(1986)
Sanders et al.
(1990)
Kasana (1991)
Kasana (1991)

Kasana (1991)
Kats et al. (1985)

Nouchi et al.
(1991)
Snyder et al.
(1991)


Runeckles et al.
(1990)





-------
                          TABLE 5-22  (cont'd).  A SUMMARY OF STUDIES REPORTING THE EFFECTS OF
I PUBLISHED SINCE U.S. ENVIRONMENTAL PROTECTION AGENCY (1986)
£ E/D/
g Species PC/Ca Concentration15 Duration
Green pepper C 19 to 66 ppb 12 h mean 77 days

Green pepper C 18 to 66 ppb 12 h mean 11 weeks

Celery C 18 to 66 ppb 12 h mean 11 weeks

Facility Variable Effect
OTC fresh fruit 12% reduction at 66 ppb.
weight
OTC fresh fruit 13% reduction in fruit
weight weight at 66 ppb.
OTC shoot dy 12% reduction at 66 ppb.
weight
Reference
Takemoto
(1988c)
Takemoto
(1988c)
Takemoto
(1988c)

et al.

et al.

et al.

E = evergreen, D = deciduous, C = crop. PC = perennial crop.
      Means are seasonal means unless specified. Maximums are 1 h seasonal maxima unless otherwise specified.  Cumulative exposures are SUMOO unless
      otherwise specified, accumulation based on 24 h/day unless otherwise noted.
^    OTC = open-top chamber with plants in ground unless specified in pots; CC = closed chamber, outside; GC = controlled environment growth chamber or
oo    CSTR; GH = greenhouse; F  = field; OF  = open-field fumigation.
      The effect reported in the study that is  a measure of growth, yield, or productivity.
      effect measured at specified ozone concentration, over the range specified under concentration, or predicted (if specified) to occur based on relationships developed
      in the experiment.

-------
 1     chambers, but was severely affected in higher concentration O3 treatments. Sanders et al.
 2     (1992) also observed yield stimulation at an 7 h growing season mean of 25 ppb (often
 3     considered background in the U.S.), however, significant yield reductions were measured as
 4     O3 concentrations increased to 50 ppb (7 h seasonal mean).
 5          A number of studies have shown soybean yields to be reduced by 10 to 15 % at 7 or
 6     12 h seasonal mean concentrations of 0.05 to 0.055 (Heagle et al., 1986b, 1987; Heggestad
 7     and Lesser, 1990; Miller et al.,  1989).
 8          A number of the studies cited above, and some of those in Table 5-22, were conducted
 9     as part of NCLAN, are considered in the  discussions of Tingey et al. (1991), Lee et al.
10     (1993a.b). and Lesser et al. (1990), but many of the experiments (primarily those not part of
11     NCLAN) were  not included in their analyses. While the range of variability in species
12     response to O3  is apparent, these studies support,  for the most part, the conclusions of U.S.
13     Environmental Protection Agency  (1986), Tingey  et al. (1991), and Lesser et al. (1990).
14     Table 5-22 summarizes the studies reporting the response of annual plants, particularly crops,
15     as growth, dry  weight, or yield  to O3 exposures (concentrations x time) under experimental
16     conditions since the previous criteria document (U.S. Environmental Protection Agency,
17     1986).  Based on the results of the studies reviewed in this section, including the reanalysis
18     of NCLAN, exposures for a three month  period to O3 concentrations currently occurring hi
19     the ambient air (0.048 to 0.06 ppm, 7  h seasonal  mean, See M7, Table 5-17) have been
20     shown to cause losses of 10% or more in the yield of the majority of major crop plants
21     grown in the country.  A number of crop species are more sensitive, and greater losses could
22     be expected (Tables 5-18 through  5-22).  It should be noted that a variety of methodologies
23     have been used to generate these data.  Generally speaking, data obtained through growth
24     chamber experiments, and experiments conducted using potted plants, may be less reliable
25     when assessing the effects of O3 than results from field growth plants.
26
27     5.6.4   Effects of Ozone on Long-Lived Plants
28           Quantifying exposure-response in the case of perennial plants (agricultural crops such as
29      pastures, alfalfa and shrubs and trees)  is complicated by they fact that they can receive multi-
30      year exposures and because the results  of exposures in a previous year, or over a number of
31      years, may be  cumulative.  Reduction in  growth and productivity, a result of altered carbon

        December 1993                          5-184      DRAFT-DO NOT QUOTE OR CITE

-------
 1      (sugar) allocation, may appear only after a number of years or when carbohydrate reserves
 2      are depleted (U.S. Environmental Protection Agency, 1986; Lawrence et al., 1993b; Garner,
 3      1991; Garner ct al., 1989).  A further complication is that in the case of evergreen plants,
 4     the life span of a leaf exceeds one year, and may be on the plant for several years.  In such
 5      cases, loss of a leaf or a reduction in photosynthetic capacity may have a large effect on a
 6     plant's ability to survive and grow.  Physiological differences among species (rates of gas
 7     exchange, for instance) may have a tendency to equalize exposure over a number of years,
 8     however,  as shown in Reich's (1987) analysis of crops, hardwoods  and conifers, and Pye's
 9     analysis of tree species  (1988). Unfortunately, there is little experimental data regarding the
10     effects of long-term O3 exposure on perennial plants, as only a few experimental studies have
11      extended exposures beyond a single growing season.  Most of what is known regarding the
12     effects of O3 on mature trees is from field observations.  Some studies that have extended
13     observation of growth alterations  into the season following exposures and thus observed
14     "carry-over effects" in several species.  Hogsett et al.  (1989) reported altered bud elongation
15     in ponderosa pine, lodgepole pine and western hemlock following a season of 03.  Altered
16     root regrowth  in ponderosa pine in the season following exposure that was correlated with
17     root storage carbohydrate was observed by Andersen et al. (1991).  Most studies have used
18     seedlings due to the difficulty of exposing large trees.   The extrapolation from seedlings to
19     large trees and to forest stands is not straight-forward,  and will, most likely, depend on the
20     use of models (Hogsett et al., 1993; Laurence et al., 1993a,b; Taylor and Hanson,  1992).
21     Correlative studies, such as those conducted in the San Bernadino mountains of California,
22     indicate potentially large impacts on ecosystems (U.S. Environmental Protection Agency,
23      1986).  This section will address three distinct types of long-lived plants: multiple-year
24     agricultural  crops, deciduous shrubs and trees, and evergreen coniferous trees.
25
26     5.6.4.1   Perennial Agricultural Crops
27           Cooley and Manning (1988) conducted a greenhouse study of the response of alfalfa to
28      O3 applied at 0.06 to 0.08 ppm for 6 h per day, 5 days a week for 8 weeks during two
29      different  years (to different plants).  Ozone treatment reduced the growth and relative growth
30      rate (by about 15 to 20% for tops and  20 to 40% for roots)  of plants before cutting, when
31      compared to a filtered-air control.  The growth of roots was more affected than the growth of

        December 1993                           5-185      DRAFT-DO NOT QUOTE OR CITE

-------
 1     tops, with a shift in the allocation pattern.  In the second year of the study, 03 exposure was
 2     continued after the plants were harvested and the impact of exposure on regrowth was
 3     determined. In this case, they found that the relative growth rate in 63 exposed plants was
 4     higher, perhaps because of an increased demand for carbon by the root systems of the
 5     Orstressed plants.  It is unclear whether these plants would sustain their increased growth,
 6     and in fact, the authors speculate that the increased growth, in lieu of partitioning carbon to
 7     other compounds, might alter the cold hardiness of the plants.
 8          Ozone has been demonstrated to affect the growth of field grown alfalfa. Temple et al.
 9     (1988a) reported a two-year study of alfalfa in which O3  at ambient concentrations (0.049 in
10     1984 and 0.042 ppm in  1985  for the seasonal 12-h means April to October) did not affect the
11     growth and yield of the  plants, but at 12 h seasonal means of 0.063 and 0.078 ppm, yield
12     was  reduced by about 15 and 19%.  The exposure-response functions for the two years were
13     homogeneous; there was no indication of cumulative effect of 03 exposure, however, crown
14     weight, an indicator of health and vigor, of exposed plants  was significantly reduced.
15          In a different field experiment conducted to determine the interactive effects of O3 and
16     simulated acid fog on stomatal conductance, photosynthesis, foliar injury, and yield of an
17     established stand of alfalfa, plants were exposed 12 h daily for 4 weeks (Temple et al.,
18      1987).  Ozone was added in proportion to its concentration in the ambient air.  Ambient
19     O3 concentrations  during the  experiment were 0.043 ppm.  Ozone injury symptoms appeared
20     on the alfalfa exposed to 0.098 ppm (NF x 2.0),  one week after the start of the regrowth
21     period.  When exposures were at 0.081  and 0.066 ppm (NF x 1.7 and NF x 1.3), more
22     than a week was required for injury to appear.  A one month exposure of the plants at the
23     end  of the growing season resulted in a  reduction of about 2.5 % in aboveground yield at a
24      12 h seasonal mean concentration of 0.04 ppm. At a concentration of 0.066 ppm, the
25      exposure resulted  in a reduction in yield of approximately  18%. It should be noted that the
26      whole plant was exposed to ambient O3  for the growing  season, only new leaves that had
27      developed after harvest received the one month exposure.  Ozone exposures could shorten
28      the productive life of alfalfa stands in addition to  its effect on yield.
 29           The sensitivity of alfalfa to O3 had been demonstrated in an earlier study using filtered
 30      air in field chambers (Neely  et al., 1977; U.S. Environmental Protection Agency, 1986).
 31      There was a 49% decrease in top dry weight when plants were exposed to 0.05 ppm,

        December 1993                           5-186      DRAFT-DO NOT QUOTE OR CITE

-------
 1     7-h/day for 68 days.  Increasing the concentration to 0.1 ppm produced a 51 % loss in dry
 2     weight at harvest.
 3          Kohul el ;il. (1988) and Hcaglc el al. (1989) experimented with forage mixtures
 4     characteristic of the northeast and southeast, respectively.  In both cases,  exposure to
 5     O3 resulted in a reduction in total forage yield of about 10 to 20% at 12 h seasonal mean
 6     O3 concentrations of 0.045 to 0.05 ppm.  In both cases, the clover component of the mix
 7     was more sensitive than the grass, and was reduced in prevalence in the stand.  The
 8     relevance of these studies to competition and species composition is  discussed in the
 9     ecosystem response section  (Section 5.7).
10          Results  of studies or perennial plants conducted since  1986 are summarized in
11     Table 5-23.   As with single-season agricultural crops, yields of multiple-year forage crops
12     are reduced at concentrations at,  or near ambient (0.04 to 0.06 ppm) in many parts of the
13     country (Table 5-17).
14
15     5.6.4.2  Effects of Ozone on Deciduous Shrubs and Trees
16          Most of the information concerning the response of deciduous  shrubs  and trees to
17     episodes, season-long, or multiple-year exposures to O3 is based on field observations.  The
18     longevity of perennial plants, and the size in the case of trees, makes experimental their
19     study under experimental conditions difficult.  For this reason, there is little experimental
20     data concerning the response of deciduous shrubs and trees.
21          Most of the hardwood experiments included in Reich's analysis (1987), for example,
22     were exposed under laboratory or greenhouse conditions to relatively high concentrations for
23     short periods of time.  Although exposures durations of weeks were conducted, square-wave
24     exposure regimes that do not capture important characteristics  of ambient exposure were
25     used.  In addition, in Pye (1988), the majority of the studies were conducted in laboratory or
26     greenhouse.  The results of a few open-top chamber studies are cited, however, the majority
27     of these studies used O3 concentrations 0.10 ppm or higher. While the studies reported in
28     Table 6-23 of U.S. Environmental Protection Agency (1986) (see Table 5-16) document the
29     sensitivity of the seedlings of some species grown in chambers, little information of value
30     with regard to  tree growth or biomass production in the long-term can be extrapolated from
        December 1993                          5.187      DRAFT-DO NOT QUOTE OR CITE

-------
December 1993









(j\
i
oo
oo



3
6
o
§
2
M
CJ
i
tn
8

O
TABLE 5-23. A SUMMARY OF STUDIES REPORTING THE EFFECTS OF
OZONE ON THE GROWTH, PRODUCTIVITY, OR YIELD OF PERENNIAL CROP PLANTS
PUBLISHED SINCE U.S. ENVIRONMENTAL PROTECTION AGENCY (1986)
Species
Strawberry

Phleum pratense

Dactylis glomerata

Poa pratensis

Festuca rubra


Festuca pratensis

Agrostis tenuis

Lolium perenne

Trifolium pratense


Plantago major

Red clover




E/D/
PC/Ca
PC

PC

PC

PC

PC


PC

PC

PC

PC


PC

PC




Concentration
18 to 66 ppb 12 h mean

10 to 55 ppb 7 h mean

10 to 55 ppb 7 h mean

10 to 55 ppb 7 h mean

10 to 55 ppb 7 h mean


10 to 55 ppb 7 h mean

10 to 55 ppb 7 h mean

62 ppb 7 h mean

6 to 59 ppb 7 h mean


70 ppb 7 h mean

19 to 62 ppb 12 h mean




Duration
1 1 weeks

5 weeks

5 weeks

5 weeks

5 weeks


5 weeks

5 weeks

5 weeks

5 weeks


8 weeks

83 and
91 days in
2 growing
seasons

Facility0
OTC

GC

GC

GC

GC


GC

GC

GC

GC


GC

OTC




Variable
fresh fruit
weight
shoot dry
weight
shoot dry
weight
shoot dry
weight
shoot dry
weight

shoot dry
weight
shoot dry
weight
shoot dry
weight
shoot dry
weight

total dry
weight
dry
weight



Effect6
20% increase in fruit
weight at 66 ppb.
45% reduction at 55 ppb.

28% reduction at 55 ppb.

28% reduction at 55 ppb.

23% reduction at 55 ppb.


16% reduction at 55 ppb.

No effect.

No effect.

30% reduction at 59 ppb.


Reduced up to 36 %
depending on growth stage.
1 1 % reduction at 62 ppb.




Reference
Takemoto et al.
(1988c)
Mortensen
(1992a)
Mortensen
(1992a)
Mortensen
(1992a)
Mortensen
(1992a)

Mortensen
(1992a)
Mortensen
(1992a)
Mortensen
(1992a)
Mortensen
(1992a)

Reiling and
Davison (1992)
Kohut et al.
(1988)




-------
 CD

 1
 u>
      Species
TABLE 5-23 (cont'd).  A SUMMARY OF STUDIES REPORTING THE EFFECTS OF
OZONE ON THE GROWTH, OR PRODUCTIVITY OF PERENNIAL CROP PLANTS
    PUBLISHED SINCE U.S. ENVIRONMENTAL PROTECTION AGENCY (1986)
 E/D/
PC/C"
             Concentration
Duration
Facility0   Variable
Effect6
                                                                                             Reference
      Timothy
      Ladino clover tall
      fescue pasture
      Ladino clover
±   Alfalfa

-------
    O
S.
          I
          W
Variable
Duration
          §
          o
          §
          U
          D.
          c/3
               oo

tv,
O
             2-
             y
growing
asons
             o
u
I*
O
                     8
                         -2
                         u
                        "

                   8 -a 8 "8

                   o «a
                       . 43
                     S C
December 1993
                    5-190     DRAFT-DO NOT QUOTE OR CITE

-------
 1      the experiments.  Trees, because of their size, are difficult to study under controlled
 2      conditions, therefore, most experiments have used seedlings in pots or in open top chambers.
 3      Since 1986, a number of studies have been conducted documenting the sensitivity of
 4      hardwoods to O3 (Table 5-24). Some species, such as black cherry,  are very sensitive
 5      (Davis and Skelly,  1992, 1992b; Simini et al., 1992), with SUM06 exposures as low as
 6      12.9 ppnvh over 92 days (concentrations not given) predicted to cause a 10% yield loss
 7      (Hogsett et al., 1993; Table 5-25).  Based on studies previously reviewed, the growth of
 8      some hardwood species, particularly those of the genus Populus, may be affected by  ambient
 9      concentrations of O3 (U.S. Environmental Protection Agency, 1978,  1986).
10          In a studies of the response of aspen clones to O3 at two field sites in Michigan,
11      Karnosky et al.  (1992a,b) documented reductions in stem weight of up to 46% in sensitive
12      aspen clones after 70 days of exposure in open-top chambers to 0.08 ppm for 6 h per day,
13      3 days per week.
14          Tjoelker and Luxmoore (1991) found leaf abscission on tulip poplar seedlings to be
15     increased by exposure to a 7 h seasonal mean concentration of 0.108 ppm, resulting  in a
16     doubling of the leaf turnover rate, but this was not translated into  an effect on growth,
17     perhaps due to the indeterminate growth habit of the plant. In such  plants, leaf production
18     continues throughout the growing season, which may permit the tree to maintain an optimal
19     leaf area.  However, continued leaf growth could deplete carbon or  nitrogen reserves.
20           Samuelson and Edwards (1993) found canopy weight of 30 year old northen red oak,
21     exposed in large open-top chambers, to be reduced by 41 % after exposure for 177 days at a
22     7-h seasonal mean of 0.069 ppm (87 ppnvh SUMOO) compared to a sub-ambient treatment at
23     a 7-h seasonal mean of 0.015 ppm  (18 ppnvh SUMOO) a concentration found nowhere in the
24     world.  Two-year old seedlings were not affected by similar exposures.
25           Hogsett et  al.  (1993) have developed exposure-response functions using uncited data for
26     aspen, red alder, black cherry, red maple, and tulip poplar (Table 5-25), as well as
27     composite functions for deciduous tree seedlings (Table 5-26).  Their results show that, for
28     28 deciduous seedling cases, a SUM06 exposure of 31.5 ppm-h over 92 days a mean
29     concentration of approximately 0.055 ppm) should result in less than a 10% yield (biomass)
30     reduction in 50% of the cases.  A 20% reduction in yield should result from a SUM06
        December 1993                          5-191      DRAFT-DO NOT QUOTE OR CITE

-------
     Almond
u.   Plum
                          TABLE 5-24.  A SUMMARY OF STUDIES REPORTING THE EFFECTS OF
                   OZONE ON THE GROWTH OR PRODUCTIVITY OF DECIDUOUS SHRUBS AND TREES
                         PUBLISHED SINCE U.S. ENVIRONMENTAL PROTECTION AGENCY (1986)
SJ
1— »
£
W





Species
Almond


Almond

E/D/
PC/Ca
D/PC


D/PC

Concentration
38 to 112 ppb 12 h mean


30 to 1 17 ppb 12 h mean

Duration
153 days


3.5 mo

Facility
OTC


OTC

Variable
total dry
weight

cross
sectional
Effect6
Linear reduction in
2 cultivars, no effect in
three.
6% reduction at 51 ppb.

Reference
Retzlaff et al.
(1992a)

Retzlaff et al.
(1991a)
     Plum
     Pear
     Apricot
    Rhus trilobata
                                                                        area
                            16 weeks in
                            each of
                            2 growing
D/PC   250 ppb 4 n/wk
D/PC   44 to 111 ppb 12 h mean   191 and
                            213 days

D/PC   30 to 117 ppb 12 h mean   3.5 mo
D/PC   30 to 117 ppb 12 h mean   3.5 mo
D/PC  30 to 117 ppb 12 h mean   3.5 mo
 D    10 to 75 ppb 12 h mean   3 mo
CC     net growth 28 and 36% reduction in
                year 1 and 2.
                                          OTC   number of  29% fewer fruit at ambient
                                                 fruit per   and above.
                                                 tree
                                          OTC   cross      19% reduction at 51 ppb.
                                                 sectional
                                                 area
                                          OTC   cross      8% reduction at 51 ppb.
                                                 sectional
                                                 area
                                          OTC   cross      53% reduction at 117 ppb.
                                                 sectional
                                                 area
                                         OTC in   growth     Increase in leaf weight in
                                          pots              ambient air.  No other
                                                           effect.
                                                                                                         McCool and
                                                                                                         Musselman (1990)
                                       Retzlaff et al.
                                       (1992b)

                                       Retzlaff et al.
                                       (1991b)

                                       Retzlaff et al.
                                       (1991b)

                                       Retzlaff et al.
                                       (1991b)

                                       Temple (1989)

-------
TABLE 5-24 (cont'd).  A SUMMARY OF STUDIES REPORTING THE EFFECTS OF
1
I— >
VO


t— '

1
1
O
1
O
<-!
OZONE ON THE GROWTH OR PRODUCTIVITY OF DECIDUOUS SHRUBS AND TREES
PUBLISHED SINCE U.S. ENVIRONMENTAL PROTECTION AGENCY (1986)
Species
Black Cherry
Black Cherry
Red Oak
Red Oak
Red Oak
Red Maple
Red Maple
Tulip Poplar
E/D/
PC/Ca
D
D
D
D
D
D
D
D
Concentration
16 to 67 ppb 12 h mean
40 or 80 ppb 7 h/day
5 days/week
18 to 87 ppnvh 15 to
69 ppb 7-h mean
16 to 67 ppb 12 h mean
40 or 80 ppb 7 h/day
5 days/week
16 to 67 ppb 12 h mean
40 or 80 ppb 7 h/day
5 days/week
16 to 67 ppb 12 h mean
Duration
3 growing
seasons
8 or 12 weeks
177 days
3 growing
seasons
8 or 12 weeks
3 growing
seasons
8 or 12 weeks
3 growing
seasons
Facility0 Variable*1
OTC growth
and leaf
dynamics
GC growth
OTC tree
canopy
OTC growth
and leaf
dynamics
GC growth
OTC growth
and leaf
dynamics
GC growth
OTC growth
and leaf
dynamics
Effect6
Leaf abscission increased
with increasing ozone.
Reduced leaf, stem, and
root dry weight, and height
at 80 ppb.
Reduced 41 % at 82 ppnvh
or 69 ppb 7-h mean.
No effect.
Reduced root dry weight at
80 ppb.
No effect.
Reduced stem diameter and
dry weight at 80 ppb.
Leaf abscission increased
with increasing ozone.
Reference
Simini et al.
(1992)
Davis and Skelly
(1992)
Samuelson and
Edwards (1993)
Simini et al.
(1992)
Davis and Skelly
(1992)
Simini et al.
(1992)
Davis and Skelly
(1992)
Simini et al.
(1992)

-------
                 TABLE 5-24 (cont'd). A SUMMARY OF STUDIES REPORTING THE EFFECTS OF
3
i-»

u>
OZONE ON THE GROWTH OR PRODUCTIVITY OF DECIDUOUS SHRUBS AND TREES
PUBLISHED SINCE U.S. ENVIRONMENTAL PROTECTION AGENCY (1986)
Species
Yellow Poplar
European Beech
Aspen
Aspen
Aspen
Yellow Poplar
Paper Birch
E/D/
PC/C* Concentration11
D 40 or 80 ppb 7 h/day
5 days/week
D 10 to 90 ppb weekly
mean
D 80 ppb 6 h/day
3 days/week
D filtered air or 80 ppb
6 h/day 3 days/week
D ambient* 27 51, or
102 ppb exposure period
mean
D 0 to 200 ppb 8 h/day
3 days/week
D 60 to 80 ppb 7 h/day
5 days/week
Duration
8 or 12 weeks
5 years
70 and
92 days in
2 growing
seasons
93 days at
2 sites in
Michigan
10S days
4.5 mo
12 weeks
Facility0 Variable*1
GC growth
OTC growth
OTC stem
weight
OTC growth
CC dry
weight
GC growth
GH dry
weight
Effect6
Reduced leaf dry weight
and stem diameter at
80 ppb.
Reduced shoot growth and
leaf area.
No effect on tolerant clones
46% reduction for sensitive
clones in one year 5%
(tolerant) and 74%
(sensitive) reductions in the
second year.
18 to 26% reduction in
diameter growth.
40% reduction— 44%
reduction in early growth
the following year.
Up to a 24% reduction at
200 ppb, but moderated by
pH treatment.
Decreased shoot and root
weight and leaf area.
Reference
Davis and Skelly
(1992)
Billen et al.
(1990)
Karnosky et al.
(1992b)
Karnosky et al.
(1992a)
Keller (1988)
Jensen and Patton
(1990)
Keane and
Manning (1988)

-------
                        TABLE 5-24 (cont'd).  A SUMMARY OF STUDIES REPORTING THE EFFECTS OF
I
VO
VO
OZONE ON THE GROWTH OR PRODUCTIVITY OF DECIDUOUS SHRUBS AND TREES
PUBLISHED SINCE U.S. ENVIRONMENTAL PROTECTION AGENCY (1986)
Species
Betula pubescens
Betula pubescens
Alnus incana
E/D/
PC/Ca
D
D
D
Concentration
25 to 82 ppb 7 h/day
25 to 82 ppb 7 h/day
25 to 82 ppb 7 h/day
Duration Facility0 Variable
50 days GC dry
weight
50 days GC dry
weight
50 days GC dry
weight
Effect*
Shoot and root dry weight
decreased linearly with
ozone.
Shoot and root dry weight
decreased linearly with
ozone.
Shoot and root dry weight
decreased linearly with
ozone.
Reference
Mortensen and
Skre (1990)
Mortensen and
Skre (1990)
Mortensen and
Skre (1990)
V  aE = evergreen, D = deciduous, C = crop, PC = perennial crop.
vo  bMeans are seasonal means unless specified. Maximums are 1 h seasonal maxima unless otherwise specified.  Cumulative exposures are SUMOO unless
     otherwise specified, accumulation based on 24 h/day unless otherwise noted.
    °OTC = open-top chamber with plants in ground unless specified in pots; CC = closed chamber, outside; GC = controlled environment growth chamber or
     CSTR; GH = greenhouse; F = field; OF = open-field fumigation.
O  ^Ths effect reported in the study mat is a measure of growth, yield, or productivity.
5  Effect measured at specified ozone concentration, over the range specified under concentration, or predicted (if specified) to occur based on relationships developed
2   in the experiment.

-------
TABLE 5-25. EXPOSURE-RESPONSE EQUATIONS THAT RELATE TOTAL
BIOMASS (FOLIAGE, STEM, AND ROOT) TO 24-HOUR SUM06 EXPOSURES (C)
ADJUSTED TO 92 DAYS (ppm-h/year)
Rate of
Growth
FAST
FAST
FAST
FAST
FAST
FAST
FAST
FAST
FAST
FAST
FAST
FAST
FAST
FAST
SLOW
SLOW
SLOW
SLOW
SLOW
SLOW
SLOW
SLOW
SLOW
SLOW
SLOW
SLOW
SLOW
SLOW
SLOW
SLOW
SLOW
SLOW
FAST
FAST
FAST
FAST
FAST
FAST
FAST
FAST
SLOW
FAST
FAST
FAST
Habit Study Species
D
D
D
D
D
D
D
D
D
D
D
D
D
D
E
E
E
E
E
E
E
E
E
E
E
E
E
E
E
E
E
E
D
D
D
D
D
D
D
D
D
D
D
D
1
1
2
2
3
3
4
4
4
4
5
5
5
6
7
7
7
7
8
8
8
9
9
10
10
10
10
11
11
11
12
13
14
15
15
16
16
17
18
19
20
21
21
22
Aspen - wild
Aspen - wild
Aspen - wild
Aspen - wild
Aspen - wild
Aspen - wild
Aspen 21 6
Aspen 253
Aspen 259
Aspen 271
Aspen 216
Aspen 259
Aspen 271
Aspen - wild
Douglas Fir
Douglas Fir
Douglas Fir
Douglas Fir
Douglas Fir
Douglas Fir
Douglas Fir
Ponderosa Pine
Ponderosa Pine
Ponderosa Pine
Ponderosa Pine
Ponderosa Pine
Ponderosa Pine
Ponderosa Pine
Ponderosa Pine
Ponderosa Pine
Ponderosa Pine
Ponderosa Pine
Red Alder
Red Alder
Red Alder
Red Alder
Red Alder
Red Alder
Black Cherry
Black Cherry
Red Maple
Tulip Poplar
Tulip Poplar
Tulip Poplar
SUM06 for Loss
Location Exposure1* Weibull Parameters of
(State) Days Year Harvests* ABC 10% 30%
OR
OR
OR
OR
OR
OR
MI
MI
MI
MI
MI
MI
MI
MI
OR
OR
OR
OR
OR
OR
OR
OR
OR
OR
OR
OR
OR
OR
OR
OR
OR
OR
OR
OR
OR
OR
OR
OR
TN
TN
TN
TN
TN
TN
84
84
118
118
112
112
82
82
82
82
98
98
98
98
113
113
234
234
118
118
230
111
111
113
113
234
234
118
118
230
140
84
121
113
113
118
118
112
76
140
55
75
184
81
1989
1989
1991
1991
1990
1990
1990
1990
1990
1990
1991
1991
1991
1991
1989-90
1989-90
1989-90
1989-90
1991-92
1991-92
1991-92
1989
1989
1989-90
1989-90
1989-90
1989-90
1991-92
1991-92
1991-92
1992
1991
1990
1989
1989
1991
1991
1992
1989
1992
1988
1990-91
1990-91
1992
1
2
1
2
1
2
1
1
1
1
1
1
1
1
1
2
3
4
1
2
3
1
2
1
2
3
4
1
2
3
1
1
1
1
2
1
2
1
1
1
1
1
3
1
9.9
17.7
31.0
75.6
67.8
96.9
54.5
73.1
79.1
91.3
37.4
35.2
35.7
19.0
16.8
27.9
33.3
83.5
26.7
85.9
119.1
12.8
25.8
12.9
25.7
32.1
90.1
20.2
47.1
44.5
134.6
136.0
42.4
84.4
206.8
63.5
248.8
54.1
53.7
37.1
28.5
45.8
334.1
150.1
96.3
165.2
130.0
124.9
111.0
142.1
121.1
265.5
92.7
44.9
128.6
95.9
73.1
263.1
462.7
3.8E+17
438.9
2887.0
109.5
-0.0058
218.7
246.9
365.2
233.7
358.8
327.8
634.3
266.4
206.5
458.5
235.8
442.8
217.0
253.0
179.9
501.7
2.0E+13
274.4
79.1
176.6
387.1
46.4
623.5
50.8
1.316 19.09
1.000 19.06
3.062 48.62
5.529 64.80
6.532 64.60
1.257 19.48
1.609 33.56
1.000 31.38
1.000 10.96
8.964 39.20
1.000 12.72
1.000 9.49
4.012 39.16
1.000 26.02
1.844 111.17
1.000 250.00
5.383 113.61
1.000 119.61
57.655 82.13
(lin) 250.00
12.254 72.80
1.000 21.56
1.000 31.89
1.000 20.05
1.000 30.77
1.000 13.58
1.000 26.27
1.000 21.88
1.000 16.96
1.257 30.61
2.570 64.56
1.000 51.10
1.427 34.08
1.000 21.70
5.294 95.76
1.000 41.21
1.000 250.00
1.107 29.50
1.123 12.91
1.168 16.90
1.537 149.75
4.518 34.56
1.000 32.85
1.852 17.12
48.21
64.54
72.41
80.79
77.86
51.40
71.60
106.23
37.10
44.91
43.06
32.11
53.07
88.08
215.37
250.00
142.49
404.91
83.88
250.00
80.42
73.00
107.95
67.87
104.18
45.97
88.94
74.09
57.42
80.77
103.76
172.98
80.10
73.46
120.57
139.51
250.00
88.79
38.23
48.00
331.07
45.27
111.19
33.07
December 1993
5-196    DRAFT-DO NOT QUOTE OR CITE

-------
            TABLE 5-25 (cont'd).  EXPOSURE-RESPONSE EQUATIONS THAT RELATE
             TOTAL BIOMASS (FOLIAGE, STEM, AND ROOT) TO 24-HOUR SUM06
                       EXPOSURES (C) ADJUSTED TO 92 DAYS (ppm-h/year)
Rate of
Growth
FAST
FAST
SLOW
SLOW
SLOW
SLOW
SLOW
Habit Study Species
E
E
D
D
E
E
E
23
23
24
24
25
25
26
Loblolly GAKR 15-91
Loblolly GAKR 15-23
Sugar Maple
Sugar Maple
E. White Pine
E. White Pine
Virginia Pine
SUM06 for Loss
Location Exposure1" Weibu» Parameters of6
(State) Days Year Harvests* A B C 10% 30%
AL
AL
MI
MI
MI
MI
MI
555
555
83
180
83
180
98
1988-89
1988-89
1990-91
1990-91
1990-91
1990-91
1992
3
3
1
3
1
3
1
22.7
20.4
4.12
24.63
0.35
1.21
78.3
4,402.5
13,125.4
100.0
110.2
63.1
719.5
3,045.1
1.000 76.89
1.000 229.24
40.069 104.79
5.987 38.68
4.191 40.90
1.000 38.74
1.000250.00
260.30
250.00
108.03
47.42
54.72
131.16
250.00
        Harvest 1 occurs immediately following end of first year of exposure. Harvest 2 occurs in spring following first year of exposure.
        Harvest 3 occurs immediately following end of second year of exposure. Harvest 4 occurs in spring following second year of exposure.
        Duration corresponds to the length in days of the first year of exposure for Harvests 1 and 2 and to the total length of the first and
        second years of exposure for Harvests 3 and 4.
        "To compare the results from seedling studies of varying exposure duration," the SUM06 value is calculated for an exposure of fixed
        period of 92 days per year. "For example, Study 1 Harvest 1 has an exposure duration of 84 days and a" SUM06 value of 19.09 ppm-h
        over 92 days which corresponds to a SUM06 value "of 19.09*84/92 = 17.43 ppm-h over 84 days, at which biomass loss is 10%." The
        calculation assumes that exposures can be scaled up or down in uniform fashion.
        Based on GIS, TREGRO and ZELIG models projections. No data given in paper.

       Source: Hogsett et al. (1993).
 1     exposure of greater than 52.1 ppm-h.  Comparison with Table 5-17 shows a SUM06 for
 2     3 mo of 29.5 ppm-h at ambient concentrations, a value near that (33.3 ppm-h) expected to
 3     prevent a 10% yield reduction in 50%  of the cases Table 5-24).  An individual year, such as
 4     1988,  might be significantly above the no-injury exposure value (Table 5-17).  By further
 5     grouping the seedlings by rate of growth (fast or slow), they were able to refine estimates of
 6     the SUM06 exposure that would protect seedlings based on growth strategy.  Deciduous
 7     seedlings and/or fast growing species are more sensitive than evergreen and/or slow growing
 8     seedlings (Table 5-24).
 9          The response of a number of fruit and nut trees to 03 has  been reported  (McCool and
10     Musselman, 1990; Retzlaff et al., 1991,  1992a,b).  Almond has been identified as the most
11     sensitive, but peach, apricot, pear, and plum have also been affected.  Net growth of
12     almond, as well as stem diameter of peach and the stem diameter and number of shoots
13     produced on apricot were reduced by four months (the exposure duration specified by the
14     authors) of once-weekly exposure to 0.25 ppm for 4 h, a relatively small exposure
15     cumulatively (16 ppm h as a SUMOO or as a SUM 06) (McCool and Musselman, 1990) but


       December 1993                            5_197      DRAFT-DO NOT QUOTE OR CITE

-------
     TABLE 5-26.  SUM06 LEVELS ASSOCIATED WITH 10 AND 20% TOTAL
         BIOMASS  LOSS FOR 50 AND 75% OF THE SEEDLING STUDIES
        (The SUM06 value is adjusted to an exposure length of 92 days per year)
Weibull Equations (all 51 seedling studies):
50th Percentile PRYL = 1 - exp(-[SUM06/176.342]**l.34962)
75th Percentile PRYL = 1 - exp(-[SUM06/104.281]**1.46719)

Weibull equations (27 fast-growing seedling studies):
50th Percentile PRYL = 1 - exp(-[SUM06/150.636]**l.43220)
75th Percentile PRYL = 1 - exp(-[SUM06/89.983]**l.49261)

Weibull equations (24 slow to moderate growing seedling studies):
501 h Percentile PRYL = I - exp(-[SUM06/190.900]**l.49986)
75th Percentile PRYL = 1 - exp(-[SUM06/172.443]**l. 14634)

Weibull equations (28 deciduous seedling studies):
50th Percentile PRYL = 1 - exp(-[SUM06/142.709]**l.48845)
75th Percentile PRYL = 1 - exp(-[SUM06/87.724]**1.53324)

Weibull equations (23 evergreen seedling studies):
50th Percentile PRYL =  1 - exp(-[SUM06/262.91 !]**!.23673)
75th Percentile PRYL =  1 - exp(-[SUM06/201.372]**1.01470)

Levels associated with prevention of a 10% and 20% total biomass loss for 50% and 75% of the seedlings.

All 51 seedling cases
                                  Percent of seedlings
                                   50%     75%
        Relative           10%      33.3     11.4
        Biomass Loss      20%      58.0     23.8

27 fast-growing seedling cases
                                  Percent of seedlings
                                   50%     75%
        Relative           10%      31.3      19.4
        Biomass Loss      20%      52.9     32.4

24 slow to moderate growth seedling cases
                                  Percent of seedlings
                                    50%      75%
        Relative            10%      42.6      24.2
        Biomass Loss      20%      70.2      46.6

 28 deciduous seedling cases
                                  Percent of seedlings
                                    50%     75%
        Relative           10%       31.5      20.2
        Biomass Loss       20%       52.1      33.0
 December 1993                            5-198      DRAFT-DO NOT QUOTE OR CITE

-------
        TABLE 5-26 (cont'd).  SUM06 LEVELS ASSOCIATED WITH 10 AND 20% TOTAL
                BIOMASS LOSS FOR 50 AND 75% OF THE SEEDLING STUDIES
              (The SUM06 value is adjusted to an exposure length of 92  days per year)	
       23 Evergreen Seedling Cases
                                      Percent of seedlings
                                       50%     75%
              Relative          10%      42.6     21.9
       	Biomass Loss	20%      78.2     45.9	

       aBased on CIS, TREGRO and ZELJG model projections. No data given in paper.
       Hogsett et al. (1993).
 1      one with a high peak value.  Cross-sectional area of almond, plum, apricot, and pear sterns
 2      decreased linearly with increasing O3, with a significant reduction at a 12 h seasonal mean of
 3      0.051; dry weight of roots, trunk, and foliage was also reduced in one variety (Retzlaff
 4      etal., 1991, 1992a,b).
 5           Finally, two studies report the response of citrus and avocado to 03 (Eissenstat et al.,
 6      1991: Olszyk et al., 1990).  These species retain their leaves for more than one year, but fit
 7      best in the deciduous category because, while evergreen, leaves are replaced more frequently
 8      than in most evergreen species.  Valencia orange trees (during a production year) exposed to
 9      a seasonal 12 h mean of 0.04 or 0.075 ppm had 11 and 31% lower yields than trees grown
10      in filtered air at 0.012 ppm and atypical concentration.  During an off-production year, yield
11      was not affected.  Growth of Ruby Red grapefruit was  not affected by concentrations of
12      3 times  ambient (Eissenstat et al., 1991).  Avocado growth was reduced by 20 or 61 % by
13      exposure during two growing seasons at 12 h seasonal mean concentrations of 0.068 and
14      0.096.
15           In summary, deciduous trees appear to be less sensitive to O3 than most crop plants,
16     but there are species that are as, or more sensitive due to their genetic composition, than
17     crops (e.g., Populus species, and perhaps black cherry—see discussion in Section 5.4.2).
18     Analysis of the crop data presented in Table 5-24 and discussed above suggests that a
19     7 h seasonal mean exposure of approximately 0.055 ppm  over a three month period would
20     prevent injury to tree seedlings. However, the absence of multiple-year studies, or  studies
       December 1993                          5499      DRAFT-DO NOT QUOTE OR CITE

-------
 1      using older, more mature trees leaves unanswered the question of long-term and cumulative
 2      effects.
 3
 4      5.6.4.3   Effects of Ozone on Evergreen Trees
 5           As with hardwoods, little long-term data from controlled studies was available at the
 6      time the literature was reviewed for U.S. Environmental Protection Agency (1986).  The
 7      1986 document did point out, however, that studies conducted on eastern white pine on the
 8      Cumberland Plateau in Tennessee indicated that ambient O3 may have reduced the radial
 9      growth of sensitive individuals as much as 30 to 50% annually over a period of 15 to
10     20 years (Mann et al., 1980).  Also, field studies in the San Bernardino National Forest
11      indicated that over a period of 30 years O3 may have reduced the growth in height of
12      ponderosa pine by as much as 25%, radial growth by 37%, and total volume of wood
13      produced by 84% (Miller et al.,  1982). Calculations of biomass in these studies were based
14     on apparent reductions in radial growth without standardization of the radial growth data with
15     respect to tree age.  Since 1986, studies on the effects of O3  on evergreen trees have focused
16     primarily on three species or groups:  red  spruce in the eastern United States, southern pines
17     (loblolly and slash), and western conifers (primarily ponderosa pine). For the most part, the
18     research has been conducted with tree seedlings or saplings, and has involved exposures
19     lasting one to four growing  seasons.  In many cases, the research  has concentrated on
20     defining the mode of action of O3 in conifers, and  is discussed elsewhere in this document
21     (Section 5.3).  Results of studies with evergreen trees are summarized in Table 5-27.
22           Hogsett et al. (1993) summarized the results from uncited data and produced composite
23     exposure-response functions for  douglas-fir,  ponderosa pine, eastern white pine, Virginia
24     pine, and loblolly pine  (Table 5-25).  They predict that a 10% loss in 50% of the
25     experimental cases  could have been prevented by a SUM06 exposure of 42.6 ppm-h
26      (O3 concentrations  and  exposure times were not given).
27           Studies of the response of  red spruce to O3 exposures,  regardless of whether they have
 28      been conducted in growth chambers  (Lee et al., 1990a,b; Patton et al., 1991; Taylor et al.,
 29      1986),  or  in the field (Kohut et  al., 1990; Laurence et al., 1993b; Thornton et  al., 1992)
 30     have failed to  detect effects on growth of seedlings or saplings, even after exposure to
 31      12  h seasonal  means of up to approximately 0.09 ppm each year for up to four years;

        December 1993                           5-200     DRAFT-DO NOT QUOTE OR CITE

-------
TABLE 5-27.  A SUMMARY OF STUDIES REPORTING THE EFFECTS OF
8
i-i




o
O
6
0
1
0
OZONE ON THE GROWTH OR PRODUCTIVITY OF EVERGREEN TREES
PUBLISHED SINCE U.S. ENVIRONMENTAL PROTECTION AGENCY (1986)
E/D/
Species PC/C Concentration
Avocado E/PC 10 to 108 ppb 12 h mean

Orange E/PC 10 to 108 ppb 12 h mean

Orange E/PC 12 to 75 ppb 12 h mean
Ponderosa Pine E ambient
Ponderosa Pine E 13 to 95 ppb 12 h mean 47
to 350 pprn-h over 3 years
Ponderosa Pine E 1 1 to 87 ppb 12 h mean
Ponderosa Pine E 5, 122 or 169 ppm-h
Ponderosa Pine E 67 to 71 ppb 7 h mean
Duration
4 and 8 mo in
2 growing
seasons
4 and 8 mo in
2 growing
seasons
7 mo/season
for 5 years
3 growing
seasons
3 growing
seasons
1 12 days
134 days
Facility0
OTCin
pots

OTCin
pots

OTC
F
OTC
OTC
OTCin
pots
OTCin
pots
Variable
leaf mass

leaf mass

fruit weight
radial
growth rate
growth
leaf weight
root growth
leaf, stem
and root
dry weight
Effect6
20 and 61 % reduction in leaf
mass at 86 and 108 ppb.

No effect.

"On" production year -
1 1 and 3 1 % reduction at
40 and 75 ppb "off year -
no effect.
No change in growth rate on
symptomatic trees.
19.5% reduction at 95 ppb.
70 and 48% loss of 2 and
1 year old needles at 87 ppb.
43 % reduction in coarse and
fine non-growing roots; 50,
65 and 62% reduction in
coarse, fine and new growing
roots.
20 to 33% reduction from
filtered air at 67 ppb.
Reference
Eissenstat et al.
(1991)

Eissenstat et al.
(1991)

Olszyk et al.
(1990)
Peterson and
Arbaugh (1988)
Beyers et al.
(1992)
Temple et al.
(1993)
Andersen et al.
(1991)
Hogsett et al.
(1989)

-------
TABLE 5-27 (cont'd). A SUMMARY OF STUDIES REPORTING THE EFFECTS OF
   OZONE ON THE GROWTH OR PRODUCTIVITY OF EVERGREEN TREES
  PUBLISHED SINCE U.S. ENVIRONMENTAL PROTECTION AGENCY (1986)
o
»— t









w>
to
8


o
E
i

2
o
H
^^
3
H
tn
O
*3
n
!-1
Species
Lodgepole Pine


Jeffrey Pine



Jeffrey Pine

Western Hemlock


Western Red Cedar


Douglas Fir


Giant Sequoia



Red Spruce


Red Spruce

E/D/
PC/Ca
E


E



E

E


E


E


E



E


E

Concentration
67 to 71 ppb 7 h mean


0-200 ppb 4 h/day
3 days/week


ambient

67 to 71 ppb 7 h mean


67 to 71 ppb 7 h mean


67 to 71 ppb 7 h mean


0-200 ppb 4 h/day
3 days/week


8 to 166 ppb 8 h mean
8 to 156 ppm-h

23 to 87 ppb 12 h mean

Duration
134 days


44 and
58 days in
2 growing
seasons
—

134 days


134 days


134 days


44 and
58 days in
2 growing
seasons
135 days


2 growing
seasons
Facility
OTCin
pots

GC



F

OTCin
pots

OTCin
pots

OTCin
pots

GC



OTC


OTCin
pots
Variable
leaf, stem
and rot
dry weight
root, stem
and
needles
dry weight
radial
growth
leaf, stem
and root
dry weight
leaf, stem
and root
dry weight
leaf, stem
and root
dry weight
root, stem
and
needles
dry weight
scion
growth

dry weight

Effect6
No effect.


Reduced 10-20% ppb in one
year.


1 1 % reduction in
symptomatic trees.
1 1 to 305 reduction at
71 ppb.

No effect.


No effect.


No effect.



No effect on juvenile or
mature scion growth.

No effect.

Reference
Hogsett et al.
(1989)

Temple (1988)



Peterson et al.
(1987)
Hogsett et al.
(1989)

Hogsett et al.
(1989)

Hogsett et al.
(1988)

Temple (1988)



Rebbeck et al.
(1992)

Kohut et al.
(1990)

-------
TABLE 5-27 (cont'd). A SUMMARY OF STUDIES REPORTING THE EFFECTS OF
CD
!
H- '
%
OJ










Ul
1
to
o
OJ


o
C
3
6
o
1
3
0
g
1
w
s
r ^
O
OZONE ON THE GROWTH OR PRODUCTIVITY OF EVERGREEN TREES
PUBLISHED SINCE U.S. ENVIRONMENTAL PROTECTION AGENCY (1986)
Species
Red Spruce

Red Spruce


Red Spruce

Red Spruce


Norway Spruce


Norway Spruce


Norway Spruce

Sitka Spruce


Silver Fir

Fraser Fir

White Pine

Loblolly Pine


E/D/
PC/Ca
E

E


E

E


E


E


E

E


E

E

E

E


Concentration
120 ppb 4 h/day
twice/week
0, 150 ppb 6 h/day or 150
ppb 6 h plus 70 ppb 18
h/day
25 or 100 ppb 4 h/day
3 day /week
27 to 54 ppb 12 h mean


80 to 100 ppb 7 to 8 h/day


14 to 70 ppb 8 h mean


10 to 90 ppb weekly mean

5 to 170 ppb 7 h/day
5 days/week

10 to 90 ppb weekly mean

20 to 100 ppb 4 h/day
3 times/week
20 to 140 ppb 7 h/day
3 day/week
21 to 86 ppb 7 h mean


Duration
4 mo

195 days


10 weeks

3 growing
seasons

100 days


5 to 6 mo in 2
growing
seasons
5 years

65 days


5 years

10 weeks

3.5 mo

96 days


Facility0
GC

GC


GC

OTCin
pots

GC


OTCin
pots

OTC

GH


OTC

GC

GC

OTCin
pots

Variable*1
growth

dry weight


growth

dry weight,
diameter,
height
dry weight


growth


growth

growth and
winter
hardiness
growth

biomass

dry weight

dry weight


Effect6
No effect.

No effect.


No effect.

No effect.


0-14% reduction vs. filtered
air - 5 provenances.

No effect.


Reduced lateral shoot growth
in last year.
No effect on growth, reduced
winter hardiness.

Increased dry matter
production.
No effect.

No effect.

18% reduction at 86 ppb
20% reduction in foliage at
40 or 86 ppb.
Reference
Taylor et al. (1986)

Patton et al. (1991)


Lee et al. (1990b)

Thornton et al.
(1992)

Mortensen (1990a)


Nast et al. (1993)


Billen et al. (1990)

Lucas et al. (1988)


Billen et al. (1990)

Tseng et al. (1988)

Reich et al. (1987)

Adams et al.
(1988)


-------
TABLE 5-27 (cont'd).  A SUMMARY OF STUDEES REPORTING THE EFFECTS OF
   OZONE ON THE GROWTH OR PRODUCTIVITY OR EVERGREEN TREES
cr
Co
w










1
to
g
^



>
H
6
O
<-*
•^
H
O
C^
O
PUBLISHED SINCE U.S.
Species
Loblolly Pine

Loblolly Pine


Loblolly Pine

Loblolly Pine

Loblolly Pine



Loblolly Pine

Loblolly Pine


Loblolly Pine

Loblolly Pine





E/D/
PC/Ca
E

E


E

E

E



E

E


E

E





Concentration
21 to 117 ppb 7 h mean

22 to 94 ppb 7 h mean


32 to 108 ppb 7 h mean

23 to 90 ppb 12 h mean 46
to 209 max 12 h
22 to 92 ppb 12 h mean 37
to 143 ppb 1 h maximum


7 to 166 ppb 12 h mean 12
h maximum 248 ppb
7 to 132 ppb 12 h mean
17 to 382 ppm-h

21 to 137 ppb 12 h mean
60 to 397 ppm-h
20 to 137 ppb 12 h mean
50 to 286 ppb maximum
12 h mean



ENVIRONMENTAL PROTECTION AGENCY (1986)
Duration
3 growing
seasons
3 growing
seasons

18 weeks

150 days

3 growing
seasons


245 days

3 growing
seasons

241 days

2 growing
seasons




Facility
OTCin
pots
OTCin
pots

OTCin
pots
OTCin
pots
OTCin
pots


OTCin
pots
OTC


OTC

OTC





Variable11
growth

dry weight


dry weight

growth

dry weight



foliar
weight
foliage
abscission

shoot
growth
needle
retention,
fascicle
length


Effect6
No effect on 5 families.

4% reduction at 30 to
38 ppb, 8% reduction at
51 to 65 ppb.
20% reduction in needles at
108 ppb.
10% reduction at 46 ppb.

0 to 13% reduction after
3 years at about 45 to 50 ppb
12 h seasonal mean,
depending on family.
35% reduction at 166 ppb.

Initiated above 130 to
220 ppm-h in trees exposed
to ambient or above.
Shoot length reduced 30% at
137 ppb.
Needle retention decreased in
elevated ozone — fascicle
length reduced by ozone in
early flushes, increased in
later flushes.

Reference
Adams et al.
(1990)
Edwards et al.
(1992)

Tjoelker and
Luxmoore (1991)
Shafer et al.
(1987)
Shafer et al.
(1989)


Qiu et al. (1992)

Stow et al. (1992)


Mudano et al.
(1992)
Kress et al. (1992)






-------
TABLE 5-27 (cont'd). A SUMMARY OF STUDIES REPORTING THE EFFECTS OF
8 OZONE ON THE GROWTH OR PRODUCTIVITY OF EVERGREEN TREES
| PUBLISHED SINCE U.S. ENVIRONMENTAL PROTECTION AGENCY (1986)
H E/D/
jg Species PC/Ca Concentration15 Duration Facility0
w Loblolly Pine E 0 to 150 ppb 5 h/day 6-12 weeks GC
5 days/week
Loblolly Pine E 0 to 320 ppb 6 h/day 8 weeks GC
4 days/week


Loblolly Pine E 0 to 120 ppb 7 h/day 12 weeks GC
5 days/week

Loblolly Pine E 0 to 320 ppb 8 h/day 9 weeks GC
4 days/week

^ Loblolly Pine E 20 to 100 ppb 4 h/day 10 weeks GC
O 3 days/week
Slash Pine E 76 to 104 ppb 7 h mean 112 days GC
126 ppb 1 h maximum
122 and 155 ppm-h
§ Slash Pine E 200 to 1 ,000 ppm-h 28 mo OTC
§
H Slash Pine E 179 to 443 ppm-h 24 h 28 months OTC
6 SUMOO multiples of
O ambient
0 .
H E = evergreen, D = deciduous, C = crop, PC = perennial crop.
O Means are seasonal means unless specified. Maximums are 1 h seasonal maxima unless
5 unless otherwise specified, accumulation based on 24 h/day unless otherwise noted.

Variable Effect6 Reference
dry weight 8% reduction at 150 ppb. Meier et al. (1990)

height and 20 % reduction in height Horton et al. (1990)
diameter growth 36% reduction in
growth diameter growth in three
open-pollinated families.
dry weight Top dry weight increased up Spence et al. (1990)
to 60 % root dry weight
reduced 6%.
relative 36% reduction in height RGR Wiselogel et al.
growth rate 10% reduction in diameter (1991)
(RGR) RGR.
dry weight No effect. Lee et al. (1990a)

top and root 18% reduction in top dry Hogsett et al.
dry weight weight and 39% reduction in (1985)
root dry weight at 122 ppm-h.
litterfall Twice as much litterfall at Byres et al. (1992)
ozone above 220 ppnrh.
leaf area Reduced up to 33 % by Dean and Johnson
443 ppm-h. (1992)



otherwise specified. Cumulative exposures are SUMOO

>-j COTC = open-top chamber with plants in ground unless specified in pots; CC = closed chamber, outside; GC = controlled environment growth
W chamber or CSTR; GH = greenhouse; F = field; OF = open-field fumigation.
O The effect reported in the study that is a measure of growth, yield, or productivity.


_ "^Effect measured at specified ozone concentration, over the range specified under concentration, or predicted (if specified) to occur based on
3 relationships developed in the experiment.
3


-------
 1      concentrations that are considerably greater than those expected in ambient air.  There was
 2      an indication that total non-structural carbohydrate content was reduced by O3, which might
 3      be an indicator of cumulative stress (Woodbury et al., 1991). However, results of these
 4      studies indicate red spruce is tolerant of O3, at least for exposures of a few years.
 5           Growth of  seedlings of loblolly pine (a much faster growing species than red spruce)
 6      has been reduced by  O3 under some conditions.  In growth chamber experiments, height
 7      growth was reduced after exposure to 0.10 ppm for 4 h per day, three days per week for
 8      10 weeks, but only in combination with a "control" rain treatment.  The effect was not
 9      observed in trees that received significant inputs of potential nutrients in simulated rain.
10     Conversely, Tjoelker and Luxmoore (1991) reported a significant reduction hi the weight of
11      current year needles  following an open-top chamber exposure to O3 at a 7 h seasonal mean
12     of 0.056 or 0.108  ppm only in a high nitrogen treatment.
13          Multiple-year open-top chamber exposures of loblolly pine have resulted in decreased
14     foliar weight, partly  through accelerated abscission, and decreased root surface area in the
15     first year following exposure to a 2.5 tunes ambient O3 treatment (0.10 ppm  12 h seasonal
16     average, 318 ppnvh) (Qiu et al.,  1992). In a two  year study, Kress et al. (1992) found that
17     fascicle length and number of early season needle flushes decreased linearly with increasing
18     O3, but the reverse was true in flushes produced later in the season.  This may only occur in
19     seedlings that produce more than two leaf flushes per year.  Foliage retention decreased with
20     O3, and fewer fascicles were retained on trees exposed to ambient concentrations of
21     O3 (12  h seasonal mean of 0.045 averaged over two years).  Shafer and Heagle (1989)
22     exposed seedlings of four families of loblolly pine to O3 over three growing  seasons and,
23     based on their data,  predicted growth suppressions of above ground plant parts at a 12 h
24      seasonal mean of  0.05 ppm of 0 to 19%  (depending on the sensitivity of the family) after two
25      years, and of 13% in the most sensitive family  after three years.  Cumulative effects of
 26      multiple-year exposures were not apparent from the above study, but no measures of root
 27      growth, which has been reported to be affected in other species (Andersen et al., 1991;
 28      Edwards et al., 1992; Temple et al., 1993) were  reported.  Edwards et al. (1992) also
 29      conducted a three year exposure and found a 4%  reduction in whole plant biomass after
 30     exposure to a 7 h seasonal concentration of about 0.050 ppm.  An 8% reduction was
        December 1993                          5-206      DRAFT-DO NOT QUOTE OR CITE

-------
 1     associated with a 7 h concentration of about 0.10 ppm. Growth reductions occurred in both
 2     above and below ground plant parts.
 3          Many studies with loblolly pine have used multiple families with a range of reported
 4     tolerance to O3 (Adams et al., 1988, 1990; Kress et al., 1992;, Qiu et al., 1992; Shafer and
 5     Heagle, 1989; Wiselogel et al.,  1991).  These studies have demonstrated the range of
 6     response, from tolerant to sensitive,  in the species.  Adams et al. (1990) suggest that
 7     resistance to natural stresses, such as drought, may be linked to tolerance to O3, thereby
 8     affecting the response of the species to multiple stresses.
 9          The response of slash pine to O3 has also been characterized. Dean and Johnson (1992)
10     found leaf area to be reduced by O3 in all three growing seasons studied, with an
11     intensification of the effect each year at an O3 exposure of about 0.03 to 0.04 ppm
12     (12 h seasonal means) or 77 to 216 ppm-h.  Leaf litterfall was also increased by O3 (Byres
13     et al.,  1992).  Volume increment of the trees was affected, with an increased  sensitivity to
14     simulated acid rain in trees exposed  to twice ambient.  Hogsett et al.  (1985) found reduced
15     height (22%), diameter (25%), top (18%), and root growth (39%) in slash pine exposed to a
16     7 h seasonal mean of 0.076 ppm, with a maximum concentration of 0.094 ppm. From these
17     studies, it is clear that slash pine is relatively sensitive to O3 on an annual basis.
18          Hogsett et al. (1989) report the results of exposing 5 western conifers to Oj at a
19     seasonal 7 h mean concentration of 0.067 or 0.071 ppm (SUM07 for 134 day was 49.5 and
20     63 ppm-h;  SUMOO was 140 and 153 ppnvh).  Ponderosa pine and western hemlock had
21     reduced needle, stem, and root dry weight after  134 days of exposure.  Douglas-fir and
22     western redcedar were not different from the charcoal-filtered air control, but douglas-fir
23     showed consistent decreases in weight of plant components. Lodgepole pine was not affected
24     by either O3 treatment.  Carry-over effects were observed in bud elongation the following
25     spring in lodgepole pine, ponderosa pine  and hemlock.  Andersen et al.  (1991) also observed
26     reduced root dry weight in ponderosa pine after exposure to SUMOO  of 122 or 169 ppnvh
27     during a 120-day growing season.  In addition, they observed a reduction in the weight of
28     newly formed roots the following spring, possibly due to reduced levels  of root starch.
29          In a three year field study, Temple et al. (1993) and Beyers et al. (1992) found that
30     ponderosa pine trees exposed to a 24 h seasonal mean of 0.087 ppm had a 48 and 70% loss
31     of 2 and 3 year old needles, respectively.  Radial stem growth and coarse root growth were

       December 1993                           5-207     DRAFT-DO NOT QUOTE OR CITE

-------
 1     also reduced, but not as severely as needle weight (due to abscission).  After three seasons of
 2     exposure, current year needles in elevated O3 treatments had a higher photosynthetic capacity
 3     than those in filtered air. The compensation was apparently due to higher foliar nitrogen in
 4     O3-exposed needles, a product of redistribution of nitrogen before abscission of needles.
 5     Cumulative responses would suggest that eventually, reductions in growth of the trees would
 6     occur at lower concentrations of O3.
 7          A number of field studies have been conducted in North America in which an attempt
 8     was made to  relate air quality to growth or injury of forest trees. Two field studies have
 9     correlated radial growth with visible injury in ponderosa and Jeffrey pine in California
10     (Peterson and Arbaugh, 1988;  Peterson et al., 1987). An 11% reduction in radial growth
11     was measured in symptomatic Jeffrey pine compared to trees that did not show  symptoms of
12     O3 injury, but no reduction could be demonstrated in ponderosa pine, however, the authors
13     point  out that the trees they measured were not under competitive stress, which might alter
14     their response.
15          The response of evergreen trees varies widely, depending on species, and genotype
16     within species.   It is clear, however, that major forest species,  such as ponderosa, loblolly,
17     and slash pine are sensitive to O3 at,  or slightly above the concentrations of O3 (0.04 to
18     0.05 ppm) that occur over wide areas of the United States.  Furthermore, because of the long
19     life span of these trees, including those that have not been reported sensitive to O3, there is
20     ample opportunity for a long-term, cumulative effect on growth of the trees.  Most of the
21     experiments  are conducted over only 2% or less of the life expectancy of the tree; an
22     equivalent exposure in field crop plants would be two to three days. Consideration must also
23     be given to the fact that most of these trees grow as part of mixed forests, in competition
24     with many other species.  Small changes in growth might be translated  into large changes in
25     stand dynamics, with concomitant effects on the structure and function of the ecosystem.
26
27      5.6.5    Assessments Using Ethylene  Diurea (EDU) as a Protectant
28           Vegetational response to air pollutants can be modified by agricultural chemicals
29      commonly used by growers to control diseases, insects and other pests on crops (see
 30      Section 5.4.7;  U.S.  Environmental Protection Agency, 1986).   A chemical protectant,
 31      ethylene diurea (EDU;  N-[2-(2-oxo-l-imidagolidinyl)ethyl]-N-phenylurea), has been used to

        December 1993                          5-208     DRAFT-DO NOT QUOTE OR CITE

-------
 1     study the response of plants to O3 without attempting to control the concentration of the
 2     pollutant during the exposure (U.S. Environmental Protection Agency, 1986) Table 5-28.
 3          Disadvantages of the use of open-top chambers for assessing the effects of Oj on the
 4     growth of plants include relatively high cost, the need for electrical power, and potential
 5     effects of the chambers themselves on the growth of the plants.  In many cases, no chamber
 6     effects can be detected, and since most studies compare against a control, chamber effects
 7     would have a minimal  effect on interpretation of results. While the number of experiments
 8     conducted with open-top chambers has led to a firm understanding of plant response to a
 9     chamber environment,  the possibility of interactions with treatment cannot be ruled out. The
10     use of EDU is attractive due to low cost and ease of application, however,  it is essential to
11     establish the correct dosage for protection from O3 without direct effects of EDU on the
12     plant, and an estimate of the level of protection from O3 achieved (Kostka-Rick and
13     Manning, 1992a,b, 1993).  EDU is known to be phytotoxic, so  studies under controlled
14     O3 conditions to establish an effective level of protection without phytotoxicity are essential
15     before it can be used as an assessment tool.
16           Previous studies with EDU led to the conclusion, as did experiments  with open-top
17     chambers,  that ambient concentrations of O3 were sufficient to reduce crop yields (U.S.
18     Environmental Protection Agency, 1986). If hourly O3 concentrations exceeded 0.08 ppm
19     for 5 to 18 days during the growing season,  yields of crops might be reduced 18 to 41 %
20     (U.S. Environmental Protection Agency, 1986).
21           Inspection of Table 5-28 shows that in many cases there were clear-cut reductions in
22     O3-induced injury, and increases in yield resulting from the application of  EDU.  However,
23     the conflicting results for field-grown soybean indicated that, at the rate of EDU application
24     used, no beneficial effects could be demonstrated.  Similarly, experiments  with corn and
25     cotton suggest that any possible effects of O3 may have been confounded by direct effects on
26     growth of  EDU itself.
27           A few studies using EDU have been conducted since 1986.  Kostka-Rick and Manning
28     (1992a,b,  1993) conducted studies to determine the direct effects of EDU on growth and to
29     develop an understanding of dose-response to EDU itself.  Their studies using EDU and
30     radish in the presence  or absence of a controlled O3 fumigation in a greenhouse and found
31     that the chemical did suppress O3-induced reductions in below-ground plant organs. It also

       December 1993                          5-209      DRAFT-DO NOT QUOTE OR CITE

-------
   u
                                                         e>o
     a
     &
I
          1"
                       1
I
                O
                        2

                        X
                               8
                                 i
December 1993
                     5-210    DRAFT-DO NOT QUOTE OR CITE

-------
                     TABLE 5-28 (cont'd).  EFFECTS OF ETHYLENE DIUREA (EDU) ON OZONE RESPONSES
u
I
      Crop/Species
                                     EDU Application
                                 O3 Exposure
                                 Effects of EDU
        Reference
Ni
      Radish (cont'd)
      Soybean
      Tobacco
      Beech
H-    Black cherry

      Other woody species:
O    Red maple
                                 Soil drench,  150 mg/1,
                                 60 ml/pot

                                 Soil drench,  500 ppm,
                                 0.51/pot
                                 Soil drench,  500 ppm,
                                 4l/6m row
Spray to runoff, 1 kg/ha
7 applications

Stem injection 1 g/1;
0.25ml

Spray to runoff, 1,000 ppm
7 applications/year

Spray to runoff, 500 ppm or
soil drench, 500 or
2,000 ppm, 250 ml/pot
                           Greenhouse, 0.07 ppm/7 h,
                           5 day/week, with two
                           weekly peaks to 0.12 ppm
                           Greenhouse; 0.2 ppm,
                           6 h/day, 2 days
                           Field; 78 h >0.12 ppm
                           (0.2 ppm max.)
Field; >0.08 ppm on
2 days

OTC; ambient and ambient
+0.08 ppm, 8 h/day

Field; 75 h >0.08 ppm
(over 4 years)

Up to 0.95 ppm, 3 h
                                                                                                                Kostka-Rick & Manning
                                                                                                                (1992b)
                           Reduced O3 injury,
                           90-100%; less reduction hi
                           hypocotyl weight
                           Reduced O3 injury, 80-90%    Brennan et al. (1987)
                                                                                      No effect on loss of
                                                                                      chlorophyll; no effect on
                                                                                      seed weight
                                                                                      Increased growth, 22%
                                                                                      No consistent effect
                                                                                      2-fold increase in growth
                                                                                      Reduced O3 injury
                                                      Smith et al. (1987) and
                                                      Brennan et al. (1990)
                                                      Bisessar and Palmer (1984)
Ainsworth and Ashmore
(1992)

Long and Davis (1991)
Cathey and Heggestad
(1982)
6
o
g
H
O
0
$
0
o
Paper birch
White ash
Honey locust
Golden-rain
London plane
Lilac
Basswood


Reduced O3 injury
Reduced O3 injury
Reduced O3 injury
Reduced O3 injury
Reduced O3 injury
Reduced O3 injury
Reduced O3 injury



-------
 1     protected the plants from foliar injury.  The EDU itself did not cause effects on growth at a
 2     concentration of 150 mg 1"  applied as a 60 ml drench to each plant, a dosage much lower
 3     than has often been used (e.g., Long and Davis,  1991; Smith, et al., 1987 discussed below).
 4     Kosta-Rick and Manning emphasize that it is essential to establish the appropriate dose for
 5     the species under consideration.  Armed with this background, they used EDU  in a field
 6     study and found an O3-induced decrease in the relative growth rates of sink organs of field-
 7     grown radish plants above a threshold level of about 0.052 to 0.058 ppm (7 h daily mean),
 8     an exposure that is near ambient O3 concentrations.
 9           EDU has also been used to estimate the effect of O3 on field-grown soybean in New
10     Jersey (Smith, et al., 1987; Brennan, et al.,  1990).  In this case, the researchers did not
11     establish the appropriate dose level for O3 protection as was  done by Kostka-Rick and
12     Manning.  No differences in  yield were found and the authors conclude that O3 does not
13     impact soybean yield of the tested cultivars in New Jersey.  However, they did not
14     demonstrate that EDU was an effective protectant at the concentrations used and on the
15     cultivars grown.
16           In a similar study, potato yields were measured and related to foliar injury in EDU
17     treated and non-treated plots over a four year period (Clarke, et al., 1990). The cumulative
18     O3 dose ranged from 45 to 110 ppm-h, depending on the year, producing a range of foliar
19     injury from 1 to 75 %.  The authors found that significant differences in yield between EDU-
20     treated and control plants occurred only  when foliar injury on untreated plants  was 75 %  of
21     leaf area.  No level of protection, other than from foliar injury, could be assessed.
22           In a three-year study of potted green ash, no significant effects on growth were
23     measured using EDU (two years) or by comparison of filtered and non-filtered air in open-
24     top chambers (one year) (Elliot, et al., 1987).  Foliar injury was observed only late in the
25      season of the first year in the non-filtered chambers.
26           An effort by Ensing, et al.  (1986) to assess the impact of Oj on yield of peanut in
 27      Ontario found that year-to-year variation was greater than that they could account for either
 28      by correlation of O3 concentration with yield of test plots or by EDU treatment.  They
 29      conclude that a correlative approach to assessing losses due to O3 will not work.
 30           Finally, a 4 year study of black cherry using EDU as  a protectant was conducted by
 31      Long and Davis (1991).  They found significant effects with a 47% reduction  in above

        December 1993                          5-212      DRAFT-DO NOT QUOTE OR CITE

-------
 1      ground biomass compared to EDU-treated trees. The authors do not believe the difference
 2      was due to a stimulation in growth due to nitrogen in the EDU, but did not conduct studies
 3      as recommended by Kostka-Rick and Manning to characterize the EDU system for black
 4      cherry.
 5           The consistency of the results on field-grown white bean in southern Ontario led to the
 6      development of an economic loss model based on the improved yields obtained as a result of
 7      applications of EDU (Adomait et al., 1987).
 8           In summary, the EDU method for assessing the impact of 03 is promising, particularly
 9      for remote areas, or as  a validation tool for existing crop-loss models.  The system must be
10      carefully characterized,  however, as pointed out by many of its users.
11           It should be noted that,  in spite of the promise shown by EDU as a field protectant over
12     many years, it has not been developed commercially, and until recently was unavailable for
13     further experimentation.
14
15     5.6.6  Summary
16          Several conclusions  were drawn from the various approaches used to estimate cropyield
17     loss.  In 1986, U.S. Environmental Protection Agency (1986) established that 7 h/day
18     growing season mean exposures to O3 concentrations above 0.05 were likely to cause
19     measurable yield loss in agricultural crops. At that tune, few conclusions could be drawn
20     about the response of deciduous or evergreen trees or shrubs because of the lack of
21     information about the response of such plants to season-long exposures to  O3 concentrations
22     of 0.04 to 0.06 ppm  and  above.  However, the 1978 and 1986 criteria documents (U.S.
23     Environmental Protection Agency, 1986) indicate that the limiting values for foliar injury to
24     trees and shrubs was 0.06 to 0.10 ppm for 4  h. Since 1986, considerable research has been
25     conducted and the sensitivity of many tree species has been established.
26           Based on research published since U.S.  Environmental Protection Agency (1986), the
27     following conclusions can be drawn:
28           1. An analysis of 10 years of monitoring data from more than  80 to almost
29             200 nonurban  sites in the U.S. established ambient 7 h growing season average
30             concentrations of O3 for 3 or 5 mo of 0.051 to  0.060 and 0.047 to 0.054 ppm,
31             respectively.  SUM06 exposures ranges from 25.8 to 45.2 ppm-h for 3 mo, and
32             32.7 to 44.4 ppm-h for 5 mo (Tingey et al., 1991).
 33

       December 1993                          5-213       DRAFT-DO NOT QUOTE OR CITE

-------
 1          2. The results of open-top chamber studies that compare yields at ambient
 2             O3 exposures with those in filtered-air, and retrospective analyses of crop data
 3             summarized in this section, establish that the current ambient concentrations of O^ at
 4             some sites are sufficient to reduce the yield of major crops in the United States.
 5             The results of research since 1978 do  not invalidate the conclusions of the U.S.
 6             Environmental Protection Agency (1976, 1986) that visible injury due to
 7             O3 exposures  reduces the market value of certain crops and ornamentals (spinach,
 8             petunia, geranium and poinsettia, for instance), and that such injury occurs at
 9             O3 concentrations (0.04 to 0.10) that presently occur in the United States.
10
11          3. A growing season SUM06 exposure of 26.4 ppm-h, corresponding to a 7 h growing
12             season mean of 0.049 ppm and a 2HDM of 0.094 ppm will prevent a  10%  loss in
13             50% of the 54 experimental cases analyzed by Tingey, et al., (1991) and Lee,  et al.,
14             (1993a,b).  A 12 h growing season  mean of 0.045  should restrict yield losses to
15             10% in major crop species (Lesser, et al., 1990).
16
17          4. Concentrations of O3 and  SUM06 exposures that occur at present  in the U.S. are
18             sufficient to affect the growth of a number of trees species.  Given the fact that
19             multiple year  exposures may cause  a cumulative effect of the growth of some trees
20             (Simini, et al., 1992; Temple, et al.,  1992), it is likely that a number of species are
21             currently being impacted, even if threshold exposures  are not being reached.
22
23          5. A study of 51 cases  of seedling response to O3 (Hogsett, et al., 1993), including
24              11 species representing deciduous and evergreen growth habits, concluded that a
25             SUM06 exposure for 5 mo of 31.5 ppm-h would protect hardwoods from a 10%
26             yield (growth) loss in 50% of the cases studied.  A SUM06 exposure of 42.6 ppm-h
27             would provide the same level of protection for evergreen seedlings.  Research  by
28             others support these conclusions. It should be noted that these conclusions do  not
29             take into the account the possibility of effects on growth in subsequent years, an
30             important consideration in the case of long-lived species.
31
32           6.  Studies of the response of trees to O3 have established that, in some cases (Populous
33              and black cherry, for instance) trees are as sensitive to O3 as annual plants, in spite
34              of the fact that they are longer lived and have lower rates of gas exchange, and
35              therefore a lower uptake of O3.
36
37           7. The use of the chemical protectant, EDU is of value to establish O3 related losses in
 38              crop yield and tree growth, providing care is exercised in establishing the
 39              appropriate dosage of the compound to protect the plants without affecting growth.
 40             EDU cannot  be used to predict the response of plants at concentrations  greater than
 41              those that exist in ambient air.

 42

 43
 44
         December 1993                          5-214      DRAFT-DO NOT QUOTE OR CITE

-------
 1      5.7   EFFECTS OF OZONE ON NATURAL ECOSYSTEMS
 2      5.7.1   Introduction
 3           The previous section presents the response of different species of crops and cultivated
 4      plants, as well as data from deciduous shrubs and trees (Table 5-25) and evergreen tree
 5      species (Table 5-26) to a variety of O3 exposure times and concentrations.  The exposure-
 6      response studies  cited in the tables in the previous section, whether conducted in chambers,
 7      greenhouses,  or open-tops suggest that all sensitive plants will respond to O3 concentrations
 8      above 0.06 ppm  within hours.  In general, depending upon the length of exposure, the
 9      number and height of peaks, and the sensitivity of the vegetation,  data from the field
10      supports this  contention.
11           The environment in both natural and agricultural ecosystems is seldom optimal for plant
12      growth. In fact,  most natural environments are suboptimal with respect to one or more
13      environmental parameters.  Plant attempting to maintain a balance of resources by integrate
14     their responses (Chapin, 1991).  Most plants undergo some form of stress during the various
15      stages of their life cycle,  however, the multiple stresses they encounter during their lifetimes
16     do not usually all occur at once.  In addition,  the sensitivity to stress varies with the age of
17     the plant (Osmond et al., 1987).  Cultivated plants are fertilized and frequently watered so
18     that they will have a balance of resources and produce better  crops. Plants growing in their
19     natural habitats must compensate not only for  the lack of resources but also for the  multiple
20     stresses they  usually encounter.  How plants respond to O3 exposures and may compensate
21     for stresses is pointed out in the section on Mode of Action (5.3).  The importance  of genetic
22     variability  in plant response, plant competition, and also the multiple biological and physical
23     factors that may  modify plant response and, in some cases cause stress, are discussed in
24     Factors That  Modify Plant Response  (5.4).  The discussion regarding modifying factors is of
25     particular importance in understanding ecosystem response to stresses because plants growing
26     in their natural habitats are much more likely  to encounter them.
27          In order to place the known plant responses to O3 exposure in the ecosystem context, a
28     brief presentation of ecosystems characteristics and their importance to human existence is
29     given in the next section.  The responses of forest ecosystems to pollutant exposure have
30     received more study than unmanaged ecosystems of other biomes (grasslands, shrublands, or
31     deserts).  The following discussion relies mainly on forest ecosystems  for its examples.

       December 1993                           5-215      DRAFT-DO NOT QUOTE OR CITE

-------
 1     5.7.2   Ecosystem Characteristics
 2     5.7.2.1  Expected Sequence of Events
 3          Ecosystems are composed of populations of "self-supporting" and "self-maintaining"
 4     living plants, animals and microorganisms (producers, consumers, and decomposers)
 5     interacting with one another and with the nonliving chemical and physical environment within
 6     which they exist (Odum, 1989; U.S. Environmental Protection Agency,  1993).  Mature
 7     ecosystems are seldom stable.  They must continually respond and adapt to changing
 8     environments (Koslowski,  1985).  Structurally complex communities, they are held in an
 9     oscillating steady state by the operation of a particular combination of biotic and abiotic
10     factors. Ecosystems usually have definable limits, the boundaries of which, and the
11     organisms that can live there, are determined by the environmental conditions of that
12     particular area or region.  They may be large or small (e.g.,  fallen logs, forests, grasslands,
13     cultivated or uncultivated fields, ponds, lakes, rivers, estuaries, oceans,  the earth) (Odum,
14     1971).  Together, the environment, the organisms, and the physiological processes resulting
15     from their interactions form the life-support systems that are essential  for the existence of
16     any species on earth, including man (Odum, 1993).
17          The importance of ecosystems to human existence is pointed out in the nitrogen oxides
18     criteria document (U.S. Environmental Protection Agency, 1993).
19          Human welfare is dependent on ecological systems and  processes.  Natural ecosystems
20     are traditionally spoken of in terms of their structure and functions. Ecosystem structure
21     includes the species  (richness and abundance) and their mass  and arrangement in an
22     ecosystem.  This is termed an ecosystem's standing stock—nature's free "goods" (Westman,
23      1977;  U.S. Environmental Protection Agency).  Society reaps two kinds of benefits from the
24     structural aspects of an ecosystem: (1) products with market value such as fish, minerals,
25     forest  products and Pharmaceuticals, and genetic resources of valuable species (e.g., plants
26     for crops and timber and animals for domestication); and (2) the use and appreciation of
27     ecosystems for recreation, aesthetic enjoyment, and study (Westman,  1977; U.S.
 28     Environmental Protection Agency).
 29           More difficult to comprehend, but no less vital, are the functional aspects of an
 30      ecosystem. They are the dynamics of ecosystems and impart to society a variety of benefits,
 31      nature's free "services".  Ecosystem  functions encompass the interactions of the ecosystem

        December  1993                          5-216      DRAFT-DO  NOT QUOTE OR CITE

-------
 1      components and their environment and maintain clean air, pure water, a green earth, and a
 2      balance of creatures; the functions that enable humans to obtain the food, fiber, energy,  and
 3      other material needs for survival (Westman, 1977; U.S. Environmental Protection Agency).
 4           Ecosystems have both structure and function.  The several most visible levels of
 5      biological organization are (1) the individual and its environment; (2) the population and its
 6      environment; (3) the community and its environment; and (4) the ecosystem (Billings, 1978).
 7      These populations of plants, animals, and microorganisms (producers, consumers and
 8      decomposers) in an ecosystem, live  together and interact as communities.  Individual
 9      organisms within a population vary  in their ability to withstand the stress of environmental
10      changes. The range of variability within which they can exist and function, determines  the
11      ability of the population to  survive.   Communities, due to the interaction of their populations,
12      respond to  pollutant stresses differently from individuals (U.S. Environmental Protection
13      Agency,  1993).
14           Intense competition among plants for light, water, nutrients, and space, along with
15      recurrent natural climatic (temperature) and biological (herbivory, disease, pathogens)
16     stresses,  can alter the species composition of communities by  eliminating those individuals
17     sensitive to specific stresses,  a common  response in communities under stress (Woodell,
18     1970; Guderian, 1985). Those organisms able to cope with stresses survive and reproduce.
19     Competition  among different species results in succession (community change over time) and
20     ultimately produces ecosystems composed of populations of plant species that have a capacity
21     to tolerate  the stresses (Kozlowski,  1980).  Pollutant stresses, such as those caused by
22     exposure to O3, are superimposed upon the naturally occurring competitional stresses
23     mentioned  above (See also Section 5.4).  Air pollutants are known to alter the diversity and
24     structure of plant communities (Guderian et al.,  1985).  The extent of change that may  occur
25     in a community depends on the condition and type of community as well as the pollutant
26     exposure.
27          In  unpolluted atmospheres, the number of species in a community usually increases
28     during succession.  Productivity, biomass, community height, and structural complexity
29     increase. Severe stresses,  on the other hand, divert energy from growth and reproduction to
30     maintenance and alter succession (Waring and Schlesinger,  1995).  In addition, biomass
31     accumulation and production decrease and structural complexity, biodiversity, environmental

       December  1993                          5-217     DRAFT-DO NOT QUOTE OR CITE

-------
 1     modification, and nutrient control are reduced (Borman, 1985).  When catastrophic
 2     disturbances or injury, whether from natural (e.g., fire, flood, or windstorm) or
 3     anthropogenic stresses (e.g., O3), alter the species composition (biodiversity) of a forest
 4     enough to disrupt food chains and modify rates of energy  flow and nutrient cycling,
 5     succession is returned to and earlier less complex stage.  The effects of stresses upon
 6     ecosystems,  unless they  are catastrophic disturbances are frequently difficult to determine
 7     (Koslowski,  1985; Garner et al., 1989).  In a mature forest, a mild disturbance becomes part
 8     of the oscillating steady  state of the forest community or ecosystem.  Responses to
 9     catastrophic  disturbances,  however, as a rule are readily observable and measurable (Garner,
10     1993).
11          The structural changes within ecosystems are the result of functional changes that
12     occurred within the individuals, populations and community (e.g., altering of nutrient cycling
13     Milleretal., 1982). Ecosystem functions include the processes and interactions among the
14     various components and their environments that involve the movement of nutrients and
15     energy through a community as organic matter. Vegetation, through the process  of
16     photosynthesis, plays and integral role in energy and nutrient transfer through ecosystems.
17     During photosynthesis, plants utilize energy from  sunlight to convert carbon dioxide (CO^)
18     from the atmosphere and water from the soil  into  carbohydrates (See Section 5.3).  The
19     energy accumulated and stored by vegetation  as carbohydrates is also available to other
20     organisms such as herbivores, carnivores, and decomposers.  As energy and nutrients move
21     from organism to organism in food chains or webs,  they become more complex as ecosystem
22     diversity increases  (Odum, 1993).  Energy flow through the food chains is unidirectional.
23     At each step some  is dissipated until ultimately, the amount left is dissipates into the
24     atmosphere as heat and must be replaced.   Nutrients and  water can be recycled, fed back into
25     the system,  and used over and over again  (Odum, 1993). The plant processes of
26     photosynthesis, nutrient uptake,  respiration, translocation, carbon allocation, and biosynthesis
27     are directly related to the ecosystem function of energy flow and nutrient cycling. Reduction
28     in structure and diversity in ecosystems shortens food chains, reduces  the total nutrient
29      inventory, and returns the ecosystems to a simpler successional stage (Woodwell, 1970).
30     How changes in  these processes influence an ecosystem is discussed in the following text.
        December 1993                           5-218      DRAFT-DO NOT QUOTE OR CITE

-------
 1     5.7.3   Ecosystem Response to Stress
 2     5.7.3.1   Forest Ecosystems
 3           Ecosystem response to  stress begins with individuals (Figure 5-23).  Individuals, not
 4     ecosystems respond to O3 exposure.  Ecosystem responses are hierarchical ranging from
 5     those that are characteristic of individuals to those characteristic of the entire ecosystem (see
 6     Section 5.7.2).  Table 5-29 lists the components that might be adversely affected by  air
 7     pollutants in  hierarchical level, the possible functional responses that might occur at  each
 8     level of organization and the associated structural changes that might be expected (Sigal and
 9     Suter, 1987). Changes in ecosystems begin with the death of individual plants.   Even though
10     ecosystems integrate individual responses and propagate them through trophic and
11     competitive relationships, there can be no ecosystem response without an individual having
12     first responded.  How the structural and functional components interact beginning with the
13     death of sensitive individuals as observed in the San Bernardino Forest  ecosystem are
14     described below.  Individuals sensitive to O3 have been described from the forests of both
15     coasts of the United States (U.S. Environmental Protection Agency,  1986). The impacts on
16     the west coast, however, have been much more severe, possibly because the exposures have
17     been chronic, continuing day and night at higher levels and the overall  O3 concentrations
18     have been  higher. In the Appalachian Mountains and the east in general O3 exposures have
19     been episodic varying in length from  days to weeks (see U.S. Environmental Protection
20     Agency, 1986).  The varying responses of the two ecosystems to O3 stress will be discussed
21     in the text that follows.
22           The extent of injury an ecosystem will experience from O3  exposure is determined by
23     the responses of its individuals.   Leaf injury, as has been stated previously, is usually the
24     first visible indication of O3  exposure.  Structural effects develop when functional responses
25     are severe enough (see Table 5-29).  Stresses,  whose primary effects occur at the molecular
26     or cellular physiology level in the individual, must be propagated progressively up through
27     more integrative levels of organ physiology (e.g.,  leaf, branch, root) to whole plant
28     physiology, stand dynamics,  and then to the landscape level to produce ecosystem effects
29     (Figure 5-24; Table 5-29).  Particularly, this is true if the stress is of low-level because only
30     a small fraction of stresses at the molecular and cellular level become disturbances at the
31     tree, stand, or landscape level.  Insect defoliation, for example, may severely reduce the

       December 1993                           5_219      DRAFT-DO NOT QUOTE OR CITE

-------
                                                                 Ozone Effects
      Atmospheric Processes
                                                                                  Other
                                                                                 Stresses
Canopy Processes
                                  Carbohydrate
                                    Allocation
 Leaf Processes/
  Ozone Uptake
                                                         Reproduction
          Leaf Processes/
          Mode of Action
                              Mineral Uptake
                                   Water Uptake
       Ecosystem Response
                                 Nitrogen
                                 Phosphoi
                                 Sulfur
                                 J     [j
Mycorrhizae Formation]
      Figure 5-23.  Effects of ozone on plant function and growth. Reduced carbohydrate
                   production decreases allocation to for resources need for plant growth
                   processes.  Solid black arrows indicate affects of ozone absorption; gray
                   stripped arrows indicate affects on plant growth.
1     growth of one or several branches while growth of the tree appears not to be affected

2     (Hinckley et al., 1992).

3          Two properties that are important in determining the effect a stress at one hierarchial

4     level of organization will have on a higher level are variability and compensation.

5     Variability in response to stress may mean that, because of genetic variation, not all trees are

6     equally susceptible.  At the stand level, the slower growth of some trees may be compensated

7     for by the relatively faster growth of others that are experiencing reduced competition so that

8     the overall growth of the stand is not affected (Hinkley et al., 1992). These properties when

9     taken together will determine the extent and rate at which stress at one hierarchical level will
       December 1993
                                      5-220
        DRAFT-DO NOT QUOTE OR CITE

-------
          TABLE 5-29. PROPERTIES OF ECOLOGICAL SYSTEMS SUSCEPTIBLE TO
                 OZONE AT FOUR LEVELS OF BIOLOGICAL ORGANIZATION
           Level of Organization
                 Properties
        Structural
          Functional Properties
        Organism
        Population
        Community
        Ecosystem
Leaf area and distribution
Biomass and allometry


Age and size structure
Population density
Genetic composition
Spatial distribution
Dispersion (spatial pattern)

Species composition
(diversity)
Trophic levels and food
webs
Physical structure (leaf area
index)

Biomass
Element pools
Soil properties
      Photosynthesis, respiration
      Nutrient uptake and release
      Carbon allocation
      Natality (reproduction,
      mortality)
      Competition
      Productivity

      Redundancy and resilience
      Succession (the integration
      of all species processes such
      as competition and
      predation)


      Ecosystem productivity
      Nutrient cycling
      Hydrologic cycling
      Energy flow
       Source:  Adapted from Sigal and Suter (1987).
 1     impact the next highest level.  To understand the effects of a stress, one must utilize the

 2     framework of hierarchical scales  (Figure 5-24) developed by Hinckley et al. (1992) to

 3     provide a means by which the effects on forest trees of the eruption of St. Helens could be

 4     followed and understood. This figure is also applicable for use when considering O3 effects

 5     and can be used to explain the difference between the response of the San Bernardino Forest

 6     ecosystem and the forests in the eastern United States.  As pointed out above, variability and

 7     compensation determine the severity of the response of the individual.

 8          Variability and compensation can also occur at the population level, all populations do

 9     not respond  equally (Taylor and Pitelka, 1992).  Plant populations can respond in four

10     different ways:  (1) no response,  the individuals are resistant to the stress; (2) mortality of all

11     individuals and local extinction of the extremely sensitive population—the most severe
       December 1993
           5-221
DRAFT-DO NOT QUOTE OR CITE

-------
                                                         Injury Symptom
                          Key Changes in Processes
                                                       Needle necrosis
                                                       & abscission

                                                       Branch length,
                                                       bifurcation ratio &
                                                       ring width growth
                                                       altered
                                                       Reduction In
                                                       diameter & death
                                                       of tree

                                                       Decreases In
                                                       stand productivity.
                                                       Increases In mortality
                                                       and alterations In
                                                       regeneration patterns
                                                                         Reduced carbon assimilation
                                                                         because of reduced radiation
                       Reduced carbon available for foliage
                       replacement & branch growth/export
                       Synerglstic Interaction between
                       mistletoe and tephra deposition
                                                                         Reduced carbon available for
                                                                         height, crown and stem growth
                       Influence of crown class on Initial
                       Impact & subsequent recovery
                       Interaction between stand
                       composition and recovery
Evaluating Impacts within a Level of Organization
Leaf Level Carbon exchange 1
Carbon pools 2
Needle #/slze 3
Needle retention/abscission 4
Branch Level Carbon allocation 5
Branch growth 6
Branch morphology 7
Branch vigor 8
Branch retention 9
Tree Level Hgt & diameter growth 1 0
Crown shape & size 1 1
Tree vigor 12
Mortality 13
Stand Level Productivity 1 4
Mortality 15
Species composition 16
    Evaluating Interactions between Different Levels of Organization
                 The diagonal arrow Indicates the Interaction between any two levels of organization.
                 The types of Interaction are due to the properties of variability, and compensation.
                 A - refers to the Interaction between the leaf and branch levels where, for example,
                    variability at the branch level determines leaf quantity and compensation at the leaf
                    level In photosynthesis may compensate for the reduction In foliage amount.
                 B- refers to the Interaction between the branch and the tree where variability In branches
                    determines Initial Interception, branch vigor and branch location In the crown, and
                    compensation may be related to Increased radiation reaching lower branches.
                 C- refers to the Interaction between the tree and the stand. Both genetic and
                    environmental variability, Inter- and Intraspecfflc compensations and tree historical
                	and competitive synerglsms Involved.	
Figure 5-24.  Effects of environmental stress on forest trees are presented on a
                hierarchial scale for the leaf, branch, tree, and strand levels of
                organization.  The evaluation of impacts within a level of organization are
                indicated by horizontal arrows. The evaluation of interactions between
                different levels of organization are indicated by diagonal arrows.


Source:  Hinckley et al. (1992).
December 1993
5-222        DRAFT-DO NOT QUOTE OR CITE

-------
 1      response; (3) physiological accommodation, growth, and reproductive success of individuals
 2      are unaffected because the stress is accommodated physiologically; and (4) differential
 3      response, members of the population respond differentially with some individuals exhibiting
 4      better growth and reproductive success due to genetically determined traits (Taylor and
 5      Pitelka, 1992). Differential  response results in the progressive elimination over several
 6      generations of the sensitive individuals and a shift in the genetic structure of the population
 7      toward greater resistance (microevolution). Physiological accommodation or microevolution,
 8      with only the latter affecting biodiversity,  are the most likely responses for exposure to
 9      chronic stress (i.e., stresses  that are of intermediate-to-low intensity and of prolonged
10     duration).  The primary effect of O3 on the more susceptible members of the plant
11      community is that the plants can no longer compete effectively for essential nutrients, water,
12     light, and space and are eliminated.  The extent of change that can occur in a community
13      depends on the condition and type of community, as well as the exposure (Garner,  1993).
14     Forest stands differ greatly in age, species composition, stability, and capacity to recover
15      from disturbance.  For this  reason, data dealing with the responses of one forest type may
16     not be applicable to another forest type (Kozlowski, 1980).
17
18     5.7.3.2   The San Bernardino Forest Ecosystem—Before 1986
19          The mixed conifer forest ecosystem  in the San Bernardino Mountains of southern
20     California is one of the most thoroughly studied ecosystems in the United States.  The
21     changes observed in the mixed conifer forest ecosystem exemplify the information presented
22     in the foregoing discussion.  Chronic O3 exposures over a period of 50 or more years caused
23     major changes in the San Bernardino National Forest  ecosystem.  The primary effect was on
24     the more susceptible members of the forest community, individuals of ponderosa and Jeffrey
25     pine, in that they were no longer able to compete effectively for essential nutrients, water,
26     light and space. As a consequence of altered competitive conditions in the community, there
27     was a decline in the sensitive species,  permitting the enhanced growth of more tolerant
28     species (Miller et al., 1982; U.S.  Environmental Protection Agency, 1978, 1986).  The
29     results of the studies  of the  San Bernardino Forest ecosystem were reported in both the 1978
30     and 1986 criteria documents (U.S. Environmental  Protection Agency, 1978, 1986). The
31     information summarized below is  from these two documents.

       December 1993                           5-223      DRAFT-DO NOT QUOTE OR CITE

-------
 1           An inventory of the forest was begun in 1968 and conducted through 1972 to determine

 2      the results of more than 30 years of exposure to O3.   Based on that inventory and

 3      accompanying studies, the conclusions reached at  that time are presented in Table 5-30.

 4      Data from the inventory indicated that for 5 mo per year from 1968 through 1972 trees were

 5      exposed to O3 concentrations greater than 0.08 ppm for more than 1300 h with

 6      concentrations rarely decreasing below 0.05 ppm  at night near the crest of the mountain

 7      slope,  elevation approximately 5,500 ft (Miller, 1973).  The importance of altitude in plant

 8      response was discussed in the 1986 criteria document (U.S. Environmental Protection

 9      Agency, 1986).

10

        	TABLE 5-30.  SAN BERNARDINO FOREST-STATUS 1972	

          1.   Ponderosa and Jeffrey pine were suffering the most  injury. Mortality of one population of ponderosa
              pine  (n =  160) was 8% Between 1969 and 1971 (p  = 0.01); in a second population (n = 40),
              mortality was 10% between 1968 and 1972.  White  fir populations had suffered slight damage, with
              scattered individual trees showing severe symptoms. Sugar pine, incense cedar, and black oak
              exhibited only slight foliar injury from oxidant exposure.

          2.   A substantial shift occurred in ponderosa pines from the  "slight injury" category in 1969 to the
               "moderate injury" category in 1971,  indicating that there was continuing oxidant stress and that the
              selective death of ponderosa pines was occurring.

          3.   Suppression of photosynthesis in seedlings was observed (Miller et al., 1969). In ponderosa pine
              saplings, needles shortened by exposure to oxidants  returned to normal length when the seedlings were
              moved to ozone-free air during 1968 to 1973 (Miller and Elderman, 1977).

          4.    Bark beetles were judged to be responsible for the death of weakened trees in the majority of cases.
               Elimination of ponderosa pine from the mixed-conifer forest was postulated to occur in the future if the
               rate  of bark beetle attack were to continue unabated (Cobb and Stark, 1970).


          5.    Aerial portions of ozone-injured pine trees showed a decrease hi vigor that was associated with
               deterioration of the feeder root system (Parameter et al., 1969).

          6.    Seed production was decreased in injured pines.  Ordinarily, trees 25 to 50 inches dbh produce the
               most cones, but they were also the most sensitive to oxidants (Luck, 1980).


          7.    Understory plant species sensitive to oxidant pollution may already have been removed by air pollution
               stress at the time of these early studies (Miller and  Elderman,  1977).


         Source: U.S. Environmental Protection Agency (1986).
         December 1993                             5-224       DRAFT-DO NOT QUOTE OR CITE

-------
 1          The survey cited above indicated the need for further information and resulted in the
 2     development of an interdisciplinary research team to more accurately determine the effects of
 3     the 30 years of exposure to O3 of the San Bernardino Forest ecosystem. The study was
 4     designed to answer two  questions:  How do organisms and biological processes of the conifer
 5     forest response to different levels of chronic oxidant exposure? and (2) How can these
 6     responses be interpreted within and ecosystem context?
 7          The research plan  included study of the limited aspects of the following ecosystem
 8     processes:  (1) carbon (energy) flow (the movement  of carbon dioxide into the plants, its
 9     incorporation into carbohydrates; and then its partitioning among, consumers, decomposers,
10     litter, and the  soil; and finally its return to the atmosphere); (2) the movement of water in the
11     soil-plant-atmosphere compartments; and (4) the shift in diversity patterns in time and space
12     as represented by changes in structure, and density in the composition of tree species in
13     communities.
14          The major abiotic  components studied were water (precipitation), temperature, light,
15     mineral nutrients (soil substrate, and oxidant pollution. The biotic components studied
16     included producers (an assortment of tree species and lichens), consumers (wildlife, insects,
17     disease organisms), and decomposers, (populations of saprophytic fungi responsible for the
18     decay of leaf and woody litter (U.S. Environmental  Protection Agency, 1978, 1986).
19           During the period of the study, 1973 to 1978,  average 24 h Qj concentrations ranged
20     from a background of 0.03 to 0.04 ppm in the eastern part of the San Bernardino Mountains
21     to a maximum of 0.10 to  0.12 ppm in the western part during May through September.
22     In addition to  total oxidant, PAN and NO2 concentrations were measured.  Peroxyacetyl
23     nitrate injury symptoms could not distinguished from O3 symptoms on herb-layer plant
24     species, while NO2 remained at non-toxic  concentrations (Miller et al., 1982; U.S.
25     Environmental Protection Agency, 1978, 1986).
26           The study indicated  that the major changes in the ecosystem began with injury to
27     ponderosa and Jeffrey pine.
28           Ponderosa pine was the most sensitive of the trees to O3 with Jeffrey pine, white fir,
29     black oak, incense cedar, and sugar pine following in decreasing order of sensitivity.  Foliar
30     injury on sensitive ponderosa and Jeffrey pine was observed when the 24-h-average
31     O3 concentrations were 0.05  to 0.06 ppm  (Miller et al., 1982).  Foliar injury, premature

       December 1993                          5-225      DRAFT-DO NOT QUOTE OR CITE

-------
 1     senescence, and needle fall decreased the photosynthetic capacity of stressed pines and
 2     reduced the production of carbohydrates needed for use in growth and reproduction by the
 3     trees.  Nutrient availability to the trees was also reduced by their retention of smaller
 4     amounts of green foliage (Miller et al., 1982). Decreased carbohydrate resulted in  a
 5     decrease in radial growth and in height of stressed trees (McBride et al., 1975; Miller and
 6     Elderman, 1977).
 7          Tree reproduction also was influenced by a reduction in carbohydrate.  Injured
 8     ponderosa and Jeffrey pines older than 130 years produced significantly fewer cones per tree
 9     than uninjured trees of the same age (Luck,  1980).  Tree ring analysis indicated declines in
10     ring width indices for many trees.  Stand thinning however reversed the trend (Miller et al.,
11     1982).
12          Summarized, the responses of individual conifers sensitive to O3 include (1) visible
13     foliar injury; (2) premature needle senescence; (3) reduced photosynthesis; (4) reduced
14     carbohydrate production and allocation; (5) reduced plant vigor; and (6) reduced growth or
15     reproduction or both (Miller et al.,  1982).  The majority of these same responses were
16     observed on  the eastern white pine growing in the Appalachian Mountains of the eastern
17     United States (McLaughlin et al., 1982; Skelly et al., 1984; U.S. Environmental Protection
18     Agency, 1986).
19          Injury to  or changes  in the functioning of other living ecosystem components  affected,
20     either directly or indirectly, the processes of carbon (energy) flow and mineral nutrient
21     cycling, water  movement and changed vegetational community patterns (Miller et al., 1982).
22     Change in decomposition patterns, altered nutrient cycling.  Early senescence and abscission
23     caused an accumulation of pine needles into a thick layer under the stands of 03 injured trees
24     and changed the successional patterns of the fungal microflora as well.  Altering the
25     taxonomic diversity and population density of the microflora that normally develop on
26      needles while they are on the tree,  influenced its relationship with the decomposer
27      community.  Change in the type of fungi on needles weakened the decomposer community
28      and the rate of decomposition (Bruhn, 1980). Carbon and mineral nutrients accumulated in
 29      the heavy  litter and the thick needle layer under stands with the most severe needle injury
 30     and defoliation and influenced nutrient availability.
        December 1993                          5-226      DRAFT-DO NOT QUOTE OR CITE

-------
 1          A comparison of lichen species found on conifers during the years 1976 to 1979 with
 2     collections from the early 1900's indicated 50% reduction in species in the more recent
 3     period.  Marked morphological deterioration of the common species Hypogymnia
 4     enteromorpha was documented in areas of high oxidant concentrations (Sigal and Nash,
 5     1983).
 6          Biotic interactions associated with predators, pathogens, and symbionts were influenced
 7     by changes in the energy available to the trees.  The decrease  in vigor and lack of ability to
 8     recover from ozone injury associated with reduced carbohydrates made the ponderosa pines
 9     more susceptible to attack by predators and pathogens (Stark and Cobb, 1969).  Dahlsten and
10     Rowney (1980) have pointed out that oxidant-weakened pines can be killed by fewer western
11     pine beetles than are required to kill healthier trees.  In stands with a high proportion of
12     O3-injured trees, a given population of western pine beetles could therefore kill more trees.
13     James et al. (1980a,b) observed that the root rot fungus, Heterobasidium annosum, increased
14     more rapidly because freshly cut stumps and roots of weakened trees were more vulnerable
15     to attack (U.S. Environmental  Protection Agency, 1986).
16           From the presentation above, it can be seen that temporal dynamics at  the level of the
17     individual organisms can upset the equilibrium  and be disorganizing in ecosystems that are
18     dominated by nonmoble organisms (Shugart, 1987). In forests with large canopy trees, a
19     canopy tree dominates the space where it is growing, reduces  the amount of light reaching
20     the forest floor and alters the microclimate, conditions that help to determine the plant
21     species that can survive beneath the canopy. Death of a canopy tree increases the resources
22     of light, nutrients, water, and  energy available to other organisms.  This change initiates a
23     struggle for dominance among understory trees and seedlings.  In time a new canopy
24     becomes established (Shugart,  1987; Garner et al., 1989).
25           The mode of death of a tree is ecologically important as it determines  the regeneration
26     success of trees that form the next forest generation.  Trees may dies catastrophically as
27     when high winds or ice storms break off the crown or branches or when they are blown
28     over, exposing roots; or they may dies slowly and tend to waste away as in  the case of those
29     injured by pathogens or insects (Shugart, 1987).  Tree death, as influenced by O3, is usually
30     gradual rather than catastrophic unless the tree is extremely sensitive or the pollutant
31     concentration is extremely high.  Growth responses require time. Therefore, because growth

       December 1993                          5_227      DRAFT-DO NOT QUOTE OR CITE

-------
1
2
3
4
5
6
responses to cumulative stresses require time and trees are continually being subjected to
many other stresses,  the cause of death is frequently difficult to determine (Garner et al.,
1989).  The continuum of vegetation changes associated with increasing pollutant stress as
seen in the San Bernardino  mixed forest ecosystem is presented in Table 5-31 (Garner et al.,
1989;  U.S. Environmental Protection Agency,  1986).


           TABLE 5-31.  ECOSYSTEM RESPONSE TO POLLUTANT STRESS
                           Stage of Response of Vegetation
                                                                  Response of Ecosystem
         Continuum

         0
         I


         n
         ra
              Anthropogenic pollutants insignificant.

              Pollutant concentrations low; no measurable
              physiological response.


              Pollutant concentrations injurious to sensitive
              species;
              (1) Reduced photosynthesis, altered carbon
                  allocation, reduced growth and vigor;
              (2) Reduced reproduction;
              (3) Predisposition to entomological or
                  microbiological stress.

              Severe pollution stress. Large plants of
              sensitive species die.  Forest layers are peeled
              off; first trees, tall shrubs and, under most
              severe conditions, short shrubs and herbs.
Unaffected; systems Pristine.

Ecosystem functions unaffected; pollutants
transferred from atmosphere to organic or
available nutrient compartments.

Altered species composition; populations of
sensitive species decline; some individuals are
lost. Their effectiveness as functional
ecosystem members diminishes; they could be
lost from the system.  Ecosystem reverts to
an earlier stage.
(1) Simplification, basic ecosystem structure
    changes, becomes dominated by weedy
    species not previously present.


(2) Reduced stability and productivity; loss
    of capability for repairing itself.  Runoff
    increases, nutrient loss, and erosion
    accelerates; a barren zone results.
    Ecosystem collapses.
        Source:  Garner et al. (1989); adapted from Bormann (1985); Kozlowski (1985); Smith (1974).
        December 1993
                                               5-228
   DRAFT-DO NOT QUOTE OR CITE

-------
 1     5.7.3.3   The San Bernardino Forest Ecosystem—Since 1986
 2          The source for pollutants transported to the mixed conifer forests of the San Bernardino
 3     Mountains is the South Coast Air Basin of southern California.  Between 1976 and 1991 the
 4     weather adjusted O3 data for the May through October "smog season"  indicates that the
 5     number of Basin days exceeding 0.12 ppm,  1 h average have declined at an average annual
 6     rate of 2.27 days per year (Davidson, 1993).  The number of days with episodes greater than
 7     0.2 ppm, 1 h average have declined at an average annual rate of 4.70 days per year over the
 8     same time period.  The total days per year with concentrations greater than 0.12 ppm was as
 9     high as  159 in 1978 with the lowest number being 105 days in 1990.  The 1974 to 1988
10     trends of the May through October hourly average and the average of monthly maximum
11     O3 concentrations for Lake Gregory, a forested area in the western section of the San
12     Bernardino Mountains, have also shown a decline (Miller et al., 1989).  Similarly there has
13     been an improvement shown in the injury index used to describe chronic injury to crowns of
14     ponderosa and Jeffrey pines between 1974 and 1988 in 13 of 15 plots located on the gradient
15     of decreasing O3 exposure in the San Bernardino Mountains (Miller et al., 1989).  The two
16     exceptions were plots located at the highest exposure end of the gradient.
17          Miller et al. (1991) reported that for the 1974 to 1988 period the basal area increase of
18     ponderosa pines was generally less than competing species at 12 of the 13 plots evaluated.
19     The total basal area for each species as percent of the total basal area for all species
20     (Figure 5-25)  shows that ponderosa and Jeffrey pines lost basal area in relation to competing
21     species that are more tolerant to  O3, namely,  white fir, incense cedar, sugar pine and black
22     oak at plots with slight to severe crown injury to ponderosa or Jeffrey pine. In effect stand
23     development has been forced in reverse, that is, the development of the normal fire climax
24     mixture dominated by fire tolerant ponderosa and Jeffrey pines is altered.  The accumulation
25     of more stems of O3 tolerant species in the understory presents a fuel ladder situation that
26     jeopardizes the remaining overstory trees in the event of a catastrophic fire. The 03 tolerant
27     species are inherently more susceptible to fire damage because of thinner bark and branches
28     close to the ground.  The important question for the future is whether the declining
29     O3 exposure will eventually allow ponderosa and Jeffrey pine  to resume dominance in basal
30     area.
        December 1993                          5-229      DRAFT-DO NOT QUOTE OR CITE

-------
          100
          80-
          80
          20
gSofTotoltt
Borrow 74 (a)
. Camp PaMka

i
I
Breezy Point



1
Sky Forest

i I, i
Schi
\
wider Creek
• II.
Dogwood

ft i Eh il
             PPICSPBO  PPWFICSPBOLO  PPWFICSPBOOW   PP JPWFSPBOQCCP  PPWFICSPBO
          100
          80-
          60
          40-
          20-
                u.c.
                Center
                                           SrfTMIUBA
                                           So(Totil74BA
                                                              (b)
                           CampAngalus
                                           Green Valley Creek
                                                     Barton Flats
                 T	1	1	1	T	n	1	1	"I	"1—-"I	"I	1	r
              PP  BO     PP WF  SP  BO     PP  JP WF  JC  SP  BO     PP  JP  SP BO  QC
          100-
           80

         r.
           20
 S of Total 74
CampOsosola
                          Holcomb Valtey
                                             Heart Bar

    (c)

Bluff Lake
               PP   JP   WF   BO
                                       JP  WF  BO
                                                          JP   WF
                                                                         JP   WF
Figure 5-25. Total basal area for each species as percent of the total basal area for all
             species in 1974 and 1988 on (a) plots with severe to moderate damage,
             (b) plots with slight damage, and (c) plots with very slight damage or no
             visible symptoms.

Source: Miller, McBride, and Schilling (1991).
December 1993
                           5-230      DRAFT-DO NOT QUOTE OR CITE

-------
 1     5.7.3.4   The Sierra Nevada Mountains
 2           Since 1991 there has been an annual survey of the amount of crown injury by 03 to the
 3     same trees in approximately 33 sample plots located in the Sierra Nevada including Tahoe
 4     National Forest, Eldorado National Forest, Stanislaus National Forest, Yosemite National
 5     Park, Sierra National Forest, Sequoi-Kings Canyon National Park, and Sequoia National
 6     Forest plus the San Bernardino National Forest.  In general, the results of this study
 7     document the regional nature of the O3 pollution problem originating primarily from the San
 8     Jaoquin Valley Air Basin (as well as the San Francisco Bay Air Basin further to the west).
 9     Oxidant air pollution is transported southward in the San Jaoquin Valley  Air Basin until it
10     reaches the southern boundary of the air basin—the Tehachipi Mountains. Because of this
11     barrier polluted air masses circulate back northward.  This circulation cell causes higher
12     O3 levels to be adverted to the southernmost administrative units, namely the Sequoia
13     National Forest and the Sequoia-Kings Canyon National Park.  The early tree injury results
14     (unpublished) corroborate the north to south increase of chronic O3 symptoms described by
15     Peterson et al.  (1991). The most important long-range object of the study is to provide a
16     data base that will allow hypothesis testing regarding exposure response of ponderosa and
17     Jeffrey pines as a function of O3 concentration statistics, summer meteorology, and stomatal
18     conductance measurements.
19           The region-wide survey (Peterson et al., 1991) of ponderosa pine provides a useful
20     backdrop for reporting a number of other studies or surveys in the Sierra Nevada that were
21     more narrowly focused.  Another tree ring analysis and crown injury  study concentrated on
22     Jeffrey pines in Sequoia-Kings Canyon National Park (Peterson et al.,  1989).  This study
23     suggested that decreases of radial growth of large, dominant Jeffrey pines growing on thin
24     soils with low moisture holding capacity and direct exposure to upslope transport of
25     O3 amounted to as much as 11 % less in recent years when compared with similar trees
26     without symptoms.
27           Both permanent plots  and cruise surveys have been employed in Sequoia, Kings Canyon
28     and Yosemite National Parks to determine the spatial distribution and temporal changes of
29     injury to ponderosa and Jeffrey pine within the Parks (Duriscoe and Stolte, 1989).
30     In Sequoia—Kings Canyon,  O3  injury to individual trees and the number of trees injured in
31     each plot increased between 1980 to 1982  and 1984 to 1985 evaluations was the most

       December 1993                          5_23i      DRAFT-DO NOT QUOTE OR CITE

-------
 1      common response among the 28 plots studied.  Ozone injury tends to decrease with
 2      increasing elevation of plots.  The O3 concentrations associated with the highest levels of tree
 3      injury in the Marble Fork drainage of the Kaweah River at approximately 1,800 m elevation
 4      are hourly averages frequently peaking at 80 to 100 ppb but seldom exceeding 120 ppb.
 5           During a cruise survey in 1986 (Duriscoe and Stolte, 1989) to identifiy the partial
 6      distribution of injury,  there were 3,120 ponderosa or Jeffrey pines evaluated for O3 injury in
 7      Sequoia, Kings Canyon and Yosemite National Parks.  Approximately one third of this
 8      number were found to have some level of chlorotic mottle.  At Sequoia, Kings Canyon
 9      symptomatic trees comprised 39% of the sample (574 out of 1,470) and at Yosemite they
10      comprised 29% (479 out of 1,650). Ponderosa pines were generally more severely injured
11      than Jeffrey pines.
12           In Sequoia, Kings  Canyon observations at field plots showed that giant sequoia
13     seedlings developed O3 injury symptoms at both ambient O3 concentrations and 1.5  X
14     ambient O3 (0.08 to 0.1 ppm hourly peaks)  (in open top chambers) during the 8 to 10 weeks
15     following germination (Miller and  Grulke, submitted).  Field plot observations of seedling
16     health and mortality in natural giant sequoia groves over a 4 year period showed that
17     seedling numbers were reduced drastically from drought and other abiotic factors.  Any
18     variable such as O3 that could stress seedlings sufficiently to reduce root growth immediately
19     after germination could increase vulnerability to late summer drought. Significant differences
20     in light compensation point, net assimilation at light saturation,  and dark respiration were
21     found between seedlings in charcoal filtered air treatments and 1.5 x  ambient O3 treatments
22      (0.08 to 0.1 ppm hourly peaks) (Grulke et al., 1989).  One interpretation of these results is
23      that O3 could be a  new selection pressure during the regeneration phase of giant sequoia,
 24      possibly reducing genetic diversity.
 25           The Lake Tahoe Basin  is located at the northern  end of the Sierra Nevada sampling
 26      transect (near the Eldorado National Forest) (Peterson  et al., 1991).  Because it is an air
 27      basin unto itself the air quality situation is distinct from other Sierra Nevada sites.  In 1987,
 28      a survey  of 24 randomly selected plots in the basin included a total of 360 trees of which
 29     105 (29.2%) had some level of foliar injury (Pedersen, 1989).  Seventeen of these plots had
 30     FPM injury scores (Pronos et al., 1978) that fell in the slight injury category.  Of 190 trees
         December 1993                          5-232      DRAFT-DO NOT QUOTE OR CITE

-------
 1     in 16 cruise plots that extended observations to the east outside the basin 21.6% had injury—
 2     less than in the basin.
 3
 4     Site  Variables Affecting Ozone Response in the California Ecosystems
 5           Structural changes in forest stands are highly related to their position on the landscape,
 6     sometimes referred to as site.  Site variables can be defined at regional and local levels.  For
 7     example,  the regional level is defined in California by the location of forested mountain
 8     slopes and summits in relation to polluted urban  air basins. In both the Sierra Nevada
 9     mountains and the San Bernardino mountains in  California the worst tree injury is found on
10     ridges that overlook the polluted air basins.  The polluted air masses are transported up-slope
11     or up-canyon in terrain that is usually sunlit in the afternoon and early  evening, thus the
12     thermal convection on warm slopes is a major means by which O3 and associated pollutants
13     are delivered to the first forested ridges. Both vertical mixing and horizontal diffusion into
14     cleaner air results in a distinct gradient  of decreasing O3  concentration  in more distant forest
15     stands. Two such gradients have been described in the San Bernardino mountains (Miller
16     et al., 1986).  Across the longer axis of the west to east orientation of  the mountain range
17     O3 concentrations range from the highest summer  months 24 h averages of 90 to 140 ppb
18     nearest the polluted South Coast Air Basin to 40 to 50 ppb at a downwind distance of 35  to
19     40 km. In the more narrow south to north direction the same concentration gradient is seen
20     over a much shorter distance of 5 to 8 km because of a more rapid transition to the warm
21     desert influence which causes mixing and dilution  (Miller et al.,  1972). Accordingly,
22     O3 injury to sensitive vegetation ranges from severe to none over these distances.
23           In the Sierra Nevada mountains a gradient  of decreasing injury is observed from west to
24     east and south to north  (Peterson and Arbaugh,  1992). But the worst level of chronic injury
25     is generally much less than  observed in the San  Bernardino mountains.
26           With respect to localized  site variables there  is evidence from repeated surveys in
27     Sequoia and Kings Canyon  National Parks that percent of trees injured and the severity of
28     foliar injury both increased  with decreasing elevation in the  1,500 to 2,500 m zone on
29     generally west facing slopes adjacent to the polluted San  Joaquin Valley Air Basin (Stolte
30     et al., 1992).  In Sequoia-Kings Canyon National Parks radial growth reductions in Jeffrey
31     pine with foliar injury by O3 was documented only for large, dominant trees growing  on

       December 1993                           5-233     DRAFT-DO NOT QUOTE OR CITE

-------
 1     shallow soils (Peterson et al., 1987).  Soil moisture availability is generally lower on such
 2     sites.  One hypothesis for explaining radial growth decline on these sites and not more
 3     favorable sites with greater moisture holding capacity is that O3 defoliation in favorable
 4     moisture years and water stress in dry years integrate sequentially to suppress growth.
 5          In the San Bernardino mountains, radial growth of ponderosa and Jeffrey pines in plots
 6     along the decreasing O3 gradient was not well correlated with level of chronic injury but was
 7     better correlated with soil moisture holding capacity.  Within a single plot with relatively
 8     uniform moisture availability there was a good correlation between increased radial growth
 9     and a decreasing level of chronic O3 visible injury to crowns.  Chappelka et al. (1992) have
10     suggested that some of the variability in foliar injury response of hardwood species to Oj in
11     Shenandoah National  Park and the Great Smoky Mountains National Park is due to elevation
12     and microsite conditions, including the proximity to streams.
13
14     5.7.3.5   The Appalachian Mountains—Before 1986
15           Oxidant induced injury on vegetation in the Applachian Mountains has been observed
16     for many years but has not produced the same ecosystem responses.  Results of studies in the
17     eastern United States was reported in the 1986 criteria document and is summarized in the
18     following passages (U.S. Environmental Protection Agency,  1986).  Needle blight of eastern
19     white pine was first reported in the early 1900s but it was not known until  1963 that it was
20     the result of acute and chronic O3 exposure (Berry and Ripperton,  1963).  The U.S. Forest
21     Service in the 1950s  studied the decline of eastern white  pine in an area covering several
22     hundred square  miles on the Cumberland Plateau in Tennessee and concluded that
23     atmospheric constituents were the cause (Berry and Hepting, 1964).  Despite this and other
24     early reports of field observations by Berry (1962, 1964), no concerted effort was  made to
25      determine the effects of O3 on the vegetation of the Appalachian Mountains until the 1970s
26      when Skelly and his  coworkers began  monitoring total oxidants and recorded associated
 27      injury to eastern white pine in three rural Virginia sites between April 1975 and March 1976
 28      (Hayes and Skelly, 1977).  Reductions in overall growth of eastern white pine was reported
 29     by Benoit (1982).  The mean ages of trees in the study plots classified as O3-tolerant,
 30     intermediate and O3-sensitive were 53, 52 and 56 years, respectively.  A comparison of
 31      growth from 1974 to 1978 with that from 1955 to 1959 based on tree rings showed decreases

        December 1993                          5-234      DRAFT-DO NOT QUOTE OR CITE

-------
  1      of 26, 37, and 51% for tolerant, intermediate and sensitive trees, respectively (Benoit, 1982).
  2      The authors assumed  the reduction in radial growth had occurred because there had been no
  3      significant changes in seasonal precipitation between the 1955 to 1959 and the 1963 to 1978
  4      periods.  Ozone concentrations for 1 h at the study cites for 1979 to 1982 ranged from a low
  5      of 0.063 ppm to a high of 0.129 ppm (U.S Environmental Protection Agency, 1986).
  6           Growth reductions in trees growing on the were studied  by Mann et al. (1980) and
  7      McLaughlin et al. (1982).  A steady growth decline in annual ring increment was observed
  8      during the years 1962 through 1979.  Reductions in average annual growth and 90% of bole
  9      growth of 70% in sensitive trees when compared to the growth of tolerant and in
10      intermediate trees were observed.  Tolerant trees consistently  showed a higher growth rate of
11      from 5 to  15% than intermediate trees for the 1960 to 1968 interval, similar growth from
12      1969 through  1975, and a reduction in growth of 5 to 15% for the period 1976 through 1979
13      when compared to trees intermediate in sensitivity.  The decline was attributed to chronic
14      O3 which frequently exceeded 1-h average  concentrations greater than 0.08 ppm. Maximum
15      1-h concentrations ranged from 0.12 to 0.20 ppm  (U.S Environmental Protection Agency,
16      1986).
17           McLaughlin et al. (1982) observed that the decline in vigor and reduction in growth in
18      trees and the production of carbohydrates (carbon flow) were  associated with the following
19      sequence of events and conditions:  (1) premature senescence  of mature needles  at the end of
20      the growing season; (2) reduced carbohydrate storage capacity in the fall and reduced
21      resupply capacity in the spring to support new needle growth; (3) increased  reliance of new
22      needles of self-support during growth;  (4) shorter  new needles, resulting in lower gross
23      photosynthetic productivity; and (5) higher  retention of current photosynthate (carbohydrate)
24      by foliage, resulting in reduced availability for transport to for external use including  repair
25      of chronically stressed tissues of older needles (U.S. Environmental Protection Agency,
26      1986).
27
28      5.7.3.6   The Appalachian Mountains—Since 1986
29          In a survey  of eastern white pine stands in the southern Appalachians fifty white pines
30      were examined for foliar symptoms (chlorotic mottle) believed to be O3-caused at 201 sites
31      distributed on a 24 x 24 km grid across the natural range  of the species in  South Carolina,

        December 1993                          5.235       DRAFT-DO NOT QUOTE OR CITE

-------
 1     Tennessee, Virginia, North Carolina, Kentucky and Georgia (Anderson et al., 1988),  The
 2     survey was conducted  from September through November 1985.  The percentage of stands
 3     with at least one symptomatic tree was highest in Kentucky (77%), followed by Tennessee
 4     (31 %), and the lowest in Georgia (10%).  The mean percentage of symptomatic trees per
 5     plot for all six states was 27 %.  The mean volume difference of 48 pairs of symptomatic and
 6     non-symptomatic trees was 49% less for symptomatic trees. Elevation and percent slope
 7     were not correlated with occurrence of symptomatic trees but most symptomatic trees were
 8     found on southwest-facing  slopes.  Plantations had  a higher percentage of symptomatic trees
 9     than did natural stands. Ozone exposure concentrations were not reported but it may be
10     possible to make estimates of exposure at the nearest O3 monitoring sites.
11          Shenandoah National Park and Great Smoky Mountains National Park are contained
12     within the survey area investigated by Anderson et al.  (1988).  These parks have been the
13     subject of several surveys for O3 injury to native vegetation. For example, Winner et al.
14     (1989) surveyed 7 to 10 individuals of 5 native species at 24 sites in Shenandoah National
15     Park. These species included tulip poplar (Liriodendron tulipifera, wild grape (Vitis sp.),
16     black locust (Robinia pseudoacacia, virgin's bower (Clematis virginiana), and milkweed
17     (Asclepias sp.).  Visible foliar injury due to O3 was most prevalent on milkweed species (up
18     to 70%) while the remaining species had injury approaching 20%.  In each case the level of
19     foliar injury increased with elevation of the sites.  The summer monthly 24-h mean
20     O3 concentrations at Blacksburg, Rocky Knob, Salt Pond and Big Meadows did not exceed
21     0.06 ppm and still foliar injury was observed.
22          Another recent survey in the Shenandoah National Park included black cherry, yellow
23     poplar, and white ash; and, in the Great Smoky Mountains National Park black cherry,
24     sassafras and yellow poplar (Chappelka et al., 1992).  Black cherry exhibited symptoms in
25     both parks. In former the percentage of leaves injured ranged from 18 to 40 while in the
26     latter the range was 8 to 29% in 1991.  Black cherry at Cove Mountain in the latter exhibited
27     the highest percentage of symptomatic trees (97%). This site also had the highest number of
28     hours exceeding 0.08 ppm.  The majority of occurrences of concentrations exceeding
29     0.08 ppm occurred during evening hours.
30           In the previous O3 document (U.S. Environmental Protection Agency, 1986f), Duchelle
31     et al. (1982, 1983) reported  that exposing native tree seedlings and herbaceous vegetation in

       December 1993                          5-236      DRAFT-DO NOT QUOTE OR CITE

-------
 1      the Big Meadows area of the Shenandoah National Park in the Blue Ridge Mountains of
 2      Virginia to ambient O3  reduced both the growth of the native trees other than eastern white
 3      pine and the productivity of the native herbaceous vegetation found growing in forested
 4      areas.  Comparison of growth of seedlings in open plots or open-top chambers with charcoal-
 5      filtered air suppressed the growth of wild-type seedlings of tulip poplar, green ash, sweet
 6      gum, black locust (Robinia pseudoacacia L.), Eastern hemlock [(tsugs canadensis (L.)
 7      Carr.), Table Mountain (Pinus pungens Lamb.), Virginia (P. virginiana Mill,) and pitch
 8      (P. rigida  Mill.) pines,  usually without visible foliar injury symptoms. Open-top chambers
 9      were operated continuously from May 9 until October 9 during the 1979 and from  April 24
10      until  September 15 in 1980 (U.S. Environmental Protection Agency, 1986).  Common
11      milkweed  (Asclepias syriaca L.) and common blackberry (Rubus allegheniensis  Porter)  were
12      two species of native vegetation to exhibit visible injury symptoms (Duchelle and Skelly,
13      1981).
14           It was mentioned previously that though there has been evidence of widespread injury
15      to native tree and other vegetation from exposure to O3 the amount of injury has not been
16      great enough for it to be transferred from the tree level to the stand level (Figure 5-23).
17      Undoubtably, there has been selection for and removal of the most sensitive tree species of
18      eastern white pine, for example.  However, the numbers of sensitive individuals in a stand
19      have  not been great enough to make a visible impact on the forest.  Simulations suggest that
20      in forests with mixed species of uneven-aged stands suggest that long-term responses are
21      likely to be shifts in species composition rather than widespread degradation (Taylor and
22      Norby, 1985; U.S. Environmental Protection Agency, 1986).
23
24      5.7.3.7   Foliage and Soil-Mediated Effects—Combined Stress
25           Previously, it has been mentioned that the environment is  seldom optimal in either
26      natural or  agricultural ecosystems.  It is not unusual, therefore, for plants growing  in natural
27      habitats to encounter multiple stresses.  Plant response to multiple stresses depend on
28      resource, particularly, carbohydrate and nitrogen, interactions at levels ranging from the cell
29      to the ecosystem (Chapin et al.,  1987). Plant responses are either foliage-mediated, soil-
30      mediated or both. The discussions in the previous section has focused on the foliaged-
31      mediated response of plant species in  an ecosystem to O3.   This section discusses the possible

        December  1993                           5.237      DRAFT-DO NOT QUOTE OR CITE

-------
 1     interactive effects of soil-mediated responses. It has usually been thought that nitrogen input
 2     to natural ecosystem alleviated deficiencies in the soil and increased plant growth (U.S.
 3     Environmental Protection Agency, 1993).  Increased nitrogen additions can lead to nutrient
 4     deficiencies of other elements (e.g., calcium and magnesium).  Aber et al., (1989) state that
 5     when nitrogen becomes readily available, other resources (e.g., phosphorus for plants and
 6     carbon for microorganisms) become limiting. Changes in nitrogen supply can have an
 7     impact on an ecosystem's nutrient balance and alter many plant and soil processes (U.S.
 8     Environmental Protection-Agency, 1993).
 9          The possible interactive effects of nitrogen on the forests of the San Bernardino
10     Mountains has come under consideration more recently. For some time there has been a
11     concern that O3 is not the only pollutant in the photochemical mixture  that may be causing
12     lasting changes in the mixed conifer forest ecosystem.  A multidisciplinary study to
13     investigate the possibility of the combined impacts on ecosystem processes from chronic
14     O3 injury and both wet and dry deposition of acidic nitrogen compounds has been under way
15     since 1991 at Barton Flats  in the San Bernardino Mountains.  The data base includes frequent
16     measurements of stomatal conductance in relation to weather and O3 exposure.
17          The nitrogen oxides criteria document  (U.S. Environmental Protection Agency, 1993)
18     explored the possible effects of increased nitrogen on litter content and decomposition.  That
19     discussion is presented here.
20           An increase in the nitrogen  litter content and  in litter decomposition rates and an
21     alteration in nitrogen cycling have been observed in the more highly polluted areas when
22     compared with moderate- and low-polluted  areas of the San Bernardino Mountains of
23     Southern California (Fenn  and Dunn,  1989). A pollutant concentration gradient exists with
24     24-h O3 concentrations at the high sites in the west averaging 0.1 ppm or higher, moderate
25     sites ranging from 0.06 to 0.08 ppm,  and low sites in the east averaging 0.05 ppm or less
26     (Fenn, 1991).  Nitrogen and sulfur compounds  also occur in the pollutant mixture to which
27     the mountains downwind of the Los Angeles Basin are exposed (Bytnerowicz et al., 1987a,b;
28      Solomon et al., 1992).  A nitrogen deposition gradient from west to east parallels the
29      decreasing O3 gradient.  Deposition of nitrogen exceeds that of sulfur (Fenn and
30     Bytnerowicz, 1992). Annual average HNO3 concentrations in 1986 ranged from 1.2 ppb
        December 1993                           5-238      DRAFT-DO NOT QUOTE OR CITE

-------
 1     near the Southern California coast to 2.7 ppb in the San Gabriel Mountains (Solomon et al.,
 2     1992).
 3          The effects of O3 exposure and injury to ponderosa (Pinus ponderosa Laws.) and
 4     Jeffrey pine (P. Jeffreyi Grev. & Balf.) on a mixed conifer forest in the San Bernardino
 5     Mountains, east of Los Angeles, have been studied for many years (Miller,  1973; Miller,
 6     1984;  U.S. Environmental Protection Agency,  1986).  The litter layers under trees severely
 7     injured by O3 is deeper than that under trees less severely injured (Fenn and Dunn, 1989).
 8     A comparison study of litter decomposition rates of L-layer litter indicates that litter from the
 9     more polluted areas  in the west decomposed at a significantly (p = 0.01) faster rate than
10     litter from moderate to low pollution levels (Fenn  and Dunn, 1989; Fenn, 1991). Nitrogen
11     content of litter was greatest at the high pollution sites and was positively correlated with the
12     litter decomposition rate.  The higher nitrogen  and lower Ca  content of the litter suggests
13     that litter hi the western plots originated from younger needles than at the less polluted sites,
14     possibly due to O3-induced needle abscission.  Fungal diversity was also greater in the litter
15     from the western San Bernardino Mountains (Fenn and Dunn, 1989).
16          When the factors associated with enhanced litter decomposition were investigated, it
17     was found that nitrogen concentrations of soil,  foliage, and litter of ponderosa and Jeffrey
18     pine were greater in the plots where pollution concentrations  were high than in moderate- or
19     low-pollution sites.  This  was also true for sugar pine (Pinus lambertiana Dougl.) and for
20     incense cedar (Calocedrus decurrens [Torr.] Florin.), two O3-tolerant species.  The rate  of
21     litter decomposition for all three pine species was  greater at the high-pollution sites.
22     Therefore, the increased rate of litter decomposition in the high-pollution plots does not
23     appear to be related to O3 sensitivity or premature needle abscission,  but rather due to higher
24     levels  of nitrogen in the soils  (Fenn, 1991).
25          Nitrogen  is the mineral nutrient that most frequently limits growth in both agricultural
26     and natural systems  (Chapin et al., 1987).  The uptake of nitrogen and its allocation is of
27     overriding importance in plant metabolism and governs, to a  large extent, the utilization of
28     phosphorus, potassium, and other  nutrients, and plant growth.  Plants usually obtain nitrogen
29     by absorbing ammonium (or ammonia) or nitrate (or  nitrite) through their roots or through
30     fixation by symbiotic organisms.   Nitrogen availability via the nitrogen cycle typically
31     controls net primary productivity.   Normally, the acquisition  of nitrogen is a major carbon

       December 1993                           5-239      DRAFT-DO NOT QUOTE OR CITE

-------
 1     expense for plants.  Plants expend a predominant fraction of the total energy available to
 2     them in the form of carbohydrates in the acquisition of nitrogen through the processes of
 3     (1) absorption, bringing nitrogen into the plant from the environment; (2) translocation,
 4     moving inorganic nitrogen within the plant; and (3) assimilation, conversion of inorganic to
 5     organic nitrogen (Chapin et al., 1987).  Absorption of nitrogen from the soil requires
 6     constant and extensive root growth to meet the needs of a rapidly growing plant because the
 7     soil pools of mineral nitrogen,  ammonium, or nitrate in the immediate vicinity of the roots
 8     are usually so small that they are quickly depleted.  A crude estimate suggests that the
 9     fraction of carbon budget spent on absorption,  translocation, and assimilation ranges from
10     25 to 45% for ammonium,  20  to 50% for  nitrate,  40 to 45% nitrogen fixation, and 25 to
11     50%  for formation of mycorrhizae (Chapin et al.,  1987).
12           Nitrogen is the mineral that most frequently  limits growth in both natural and
13     agricultural ecosystems (Chapin et al., 1987).  The uptake of nitrogen and its allocation is of
14     overriding importance in plant  metabolism and governs, to a large extent, the utilization of
15     phosphorus,  potassium, and other nutrients, and plant growth.  Nitrogen availability via the
16     nitrogen cycle typically controls  net primary productivity.  Normally, the aquisition of
17     nitrogen is a major carbohydrate expense for plants.
18           Nitrogen uptake influences photosynthesis because in the leaves of plants with
19     C3 photosynthesis (the pathway used by most of the world's plants), approximately 75% of
20     the total nitrogen is contained in the choloroplasts and is used during photosynthesis.  The
21     nitrogen-photosynthesis relationship is, therefore,  critical to the growth of trees (Chapin
22     et al., 1987). As a rule,  plants allocate resources most efficiently when growth is  equally
23     limited by all resources.  When a specific  resource such as nitrogen limits growth, plants
24     adjust by allocating carbohydrates to the organs that acquire the most strongly limiting
25     resources (Figure 5-26).
26           Among boreal and subalpine conifers, nitrogen added to the soil may not increase
27      growth.  Depending on the plant species,  nitrogen use efficiency above a critical level
28      decreases.  All plants do not necessarily benefit from the added nitrogen in the leaves. More
29      nitrogen in the soil is not mirrored directly by increased nitrogen uptake except at  low levels.
30      This is particularly true of conifers that are adapted to low-resource environments and tend to
31      have low potential growth rates.  The photosynthetic capacity of conifer foliage is  low and

        December 1993                            5-240     DRAFT-DO NOT QUOTE OR CITE

-------
                                      Leaf
                                    Biomass
Photosynthetic
    Rate
c    /
  " K \
           Root
          Biomass
                                                     Nutrient \
                                                     Uptake )
          Initial
          Allocation
          State
          Environmental
          Stress
                                                      Carbon
Reduce Carbon Supply
     Low Light
     SOj/Og
                        Leaf
                       Biomass
       Reduce Nitrogen/Water Supply
                Drought
             Low Soil Fertility
                                                           Root
                                                         Biomass
          New
          Allocation
          State                	           	                   -*^_«
                                   "Carbon-   "^                   ^" —Carbon'
       Figure 5-26.  Impact of a reduced supply of carbon to the shoot, or water and nitrogen
                     t(> the roots, on  subsequent allocation of carbon.
       Source: Winner and Atkinson (1986).
 1     not greatly enhanced by increased nitrogen content (Waring, 1985; Chapin, 1991).  High leaf
 2     nitrogen content is not always an advantage when other resources, among which are light and
 3     water, are limited.  At the present time, data dealing with the response of trees or other
 4     vegetation to the combined stresses of O3 exposure above ground and nitrate deposition
 5     through the soil are sparse.  Tjoelker and Luxmoore (1991), however, have assessed the
 6     effects of soil nitrogen availability and chronic O3 stress on carbon and nutrient economy in
 7     1-year-old seedlings of loblolly pine (Pinus taeda L.) and yellow poplar (Liriodendron
 8     tulipifera L).  Elevated O3 concentrations altered biomass partitioning to needles of the
 9     current year.  Ozone concentrations of 0.108 ppm reduced the biomass of current-year
10     needles in loblolly pine seedlings grown at the highest (172 ^tg/g) nitrogen supply by 20%,
11     but not those grown with a low (59 jug/g) supply of nitrogen.  The interaction between
12     O3 and nitrogen suggests that plants grown with a high nitrogen supply are more sensitive to
13     chronic O3 stress in terms of biomass reduction (Tjoelker and Luxmoore, 1991). Similar
14     results in the growth of domestic radish  (Raphanus saliva L., cv. Cherry Bell) were obtained
15     by Pell et a). (1990).  Brewer et al. (1961) and Harkov and Brennan (1980) observed
       December 1993
                     5-241
DRAFT-DO NOT QUOTE OR CITE

-------
 1     increased foliar injury when plants were grown with an adequate nitrogen supply (U.S.
 2     Environmental Protection Agency).
 3
 4     5.7.3.8   Mycorrhizae-Plant Interactions
 5          Mycorrhizae are quite literally, "fungus-roots", an association between plant roots and
 6     fungi that is beneficial to both.  The majority of plants develop this relationship and could
 7     not reach optimum growth  without it. Mycorrhizal fungi increase the uptake of mineral
 8     nutrients for the host plants, protect roots against pathogens, produce plant growth hormones,
 9     and move carbohydrates from one plant to another (Hacskaylo, 1972).  The fungi in return
10     receive food in the form of simple sugars from the plant roots. Ozone has the capability of
11     disrupting the association between the mycorrhizal  fungi and host plants by  inhibiting
12     photosynthesis and reducing the amount of sugars available for transfer from the shoots to
13     the roots (see Figure 5-25). The benefits of this relationship was discussed in the previous
14     criteria document (U.S. Environmental Protection Agency, 1986).
15          Mycorrhizal  fungi are an  integral part of the below-ground ecosystem  of terrestrial
16     communities.  Some plants appear to be obligately mycorrhizal, while others are facultative
17     or non-mycorrhizal; however, mycorrhizae form on the vast majority of terrestrial plants and
18     contribute substantially to ecosystem function (Allen, 1991; Harley and Smith, 1983).  The
19     symbiotic association is mutually beneficial and is characterized by a flow of nutrients from
20     fungus to host and flow of carbohydrates from host to fungus.  Since oxidants have been
21     shown to alter photosynthesis and carbohydrate allocation  within the plant, often decreasing
22     allocation to  roots, they can disrupt the association by reducing carbohydrate availability to
23     the fungus.  Any change in the vigor of the association will influence the nutrient harvesting
24     capability of the mycorrhizal hyphae, the physiology of the host plant, and subsequently
25     ecosystem function.
26           Several  studies of the effects of 03 on tree species have included investigations of the
27     effects on ectomycorrhizal associations. The topic has been discussed in a series of articles
28     in a special issue of the journal Environmental Pollution (Vol. 73,  No. 2), and selected
29     studies are summarized in  Table  5-32. The understanding of oxidant effects on root
30     symbioses has not changed substantially since 1986 (U.S.  Environmental Protection Agency,
31      1986), however, understanding of the importance of symbiotic organisms in ecosystem

       December 1993                          5-242       DRAFT-DO NOT QUOTE OR CITE

-------
           TABLE 5-32.  INTERACTIONS OF OZONE AND FOREST TREE ECTOMYCORRHIZAE INTERACTIONS
 3
 8*
 u>
Host Plant
    Mycorrhizae       Exposure Condtions     Effect of O3 on Mycorrhiza
                                                          Reference
Ul
to
     Loblolly pine
Scots pine
White pine
Norway Spruce

Paper Birch
Red Oak
Pisolithus tinctorius
not stated
not stated
not stated
10 spp.
Pisolithus tinctorius
6 spp.
4 spp.
Pisolithus tinctorius
not stated
OTC, field             reduced root infection
OTC, field, 3 years      reduced root infection
CEC                   no effect
CSTR                  reduced root infection
open air, field, 3 years   no significant effects
CEC                   reduced root infection
open air, field, 3 years   no significant effects
CEC                   no consistent effects
CEC                   no effects
CEC and OTC          significant increase
Adams and O'Neill (1991)
Edwards and Kelly (1992)
Mahoney et al. (1985)
Meier et al. (1990)
Shaw et al. (1992)
Stroo et al. (1992)
Shaw et al. (1992)
Blaschke and Weiss (1990)
Keane and Manning (1988)
Reich et al. (1985)
     CEC: controlled environment chamber; CSTR: continuous stirred tank reactor; OTC: open-top filed chamber.
I
§

-------
 1     function has improved.  The basic hypothesis on mechanisms remains the same (i.e., effects
 2     are mediated through host carbohydrate metabolism) since oxidants do not penetrate the soil
 3     more than a few centimeters. Most of the research has been conducted on individual plant
 4     species in controlled environments, and while the role of mycorrhizae in community stmcture
 5     has been recognized, it has not specifically been addressed experimentally. Below is a
 6     review of recent studies addressing oxidants  effects on mycorrhizae.
 7          Several studies have refined our understanding of oxidant stress effects on roots.
 8     In Pseudotsuga menziesii [Mirb.] Franco root/soil respiration was significantly reduced
 9     during the first 1 to 2 weeks after exposure to O3  or SO2, followed by a recovery period
10     which resulted in similar total respiratory release between treatments and controls (Gorissen
11     and Van Veen, 1988;  Gorissen et al.,  1991). Total allocation to roots did not appear to be
                                                                                14
12     reduced, but 03 apparently reduced translocation to roots in that respiration of   C was
13     suppressed.   Edwards (1991) found that root and soil respiration were reduced in Pinus
14     taeda L. seedlings exposed to O3 levels ranging from 0.07 to 0.11 ppm (7 h mean) compared
15     to seedlings exposed to levels below ambient (0.02 to 0.04 ppm).  Nouchi et al. (1991) found
16     that 03 at 0.1 ppm reduced root respiration by 16% in Oryza. sativa L. after one week of
17     exposure. However, exposure to 3 to 7 weeks of 0.1 ppm O3 resulted in elevated levels of
18     root respiration.
19           Several studies have examined the effects of O3 on carbohydrate allocation to roots and
20     subsequent shifts in biomass allocation (Cooley and Manning, 1987; Kostka-Rick and WJ.
21     Manning, 1992; Karnosky et al., 1992; Temmerman, Vandermeiren and Guns, 1992; Qui
22     et al., 1992; Sharpe et al., 1989; Gorissen and Van Veen, 1988; Gorissen et al., 1991;
23     Spence et al., 1990).  Gorissen et al. (1991) examined the combined effects of 03 and
24     ammonium sulfate application to Psuedotsuga menziesii [Mirb.] Franco in association with
25     Khizopogon vinicolor A.H. Smith and Lactarius rufus (Scop. :Fr.)Fr.  They found greater
26     needle retention of 14C labelled compounds in the new needles of O3 treated plants, and a
27     trend towards less 14C labelled substrates  recovered in roots and root/soil fractions.
28     Short-term transport of UC labelled substrates were followed throughout P. taeda (Spence
29     et al., 1990). A 45% reduction in transport of photosynthates to roots occurred in O3 treated
30     plants compared to controls.  Collectively, the studies have  shown a general trend of
31     diversion of carbohydrate resources from roots and retention in the photosynthetically active

       December 1993                           5-244     DRAFT-DO NOT QUOTE OR CITE

-------
 1      portions of plants.  A reduction in allocation to roots may be associated with a change in the
 2      availability of carbohydrate for maintenance of root symbioses.
 3           The effects of O3 on mycorrhizal colonization have varied depending on the
 4      experimental conditions and the species used.  Stroo et al. (1988) studied the effects of 03 on
 5      mycorrhizal infection in Pinus strobus seedlings grown for 4 mo in several soils.  Results
 6      varied by soil type and nitrogen availability; however, in several soils the number of
 7      mycorrhizal short roots increased slightly at low O3 levels and decreased  significantly at
 8      higher O3  concentrations.  Reich et al. (1986)  found similar results in P.  strobus L. and
 9      Quercus rubra L., and concluded that O3 may stimulate mycorrhizal infection at low
10      O3 concentrations. Simmons and Kelly (1989) observed a trend of greater mycorrhizal short
11      roots in Pinus taeda seedlings exposed to subambient O3  treatment than those exposed to
12      ambient or twice ambient O3 levels; results were not statistically significant.  In another
13      study with two families of P. taeda, Adams and O'Neill (1991) found that mycorrhizal
14      colonization tended to increase with O3 during the first 6 weeks of exposure, and decrease
15      with O3 after 12 weeks of exposure.  Meier et al.  (1990) found a decrease in ectomycorrhizal
16      root tips and percentage of feeder roots in P. taeda L. seedlings.  Keane  and Manning (1988)
17      found significant interactions among O3, soil type and pH, however the direct effects of
18      O3 were difficult to elucidate.  Collectively, these  results suggest that O3  does impact
19      colonization of roots by mycorrhizal fungi; however the results illustrate the variability in
20      response due to such factors as soil condition,  duration of experiment, and timing of
21      measurements.
22           Altered root carbohydrate allocation resulting from O3 exposure may affect host-fungus
23      compatibility (Edwards and Kelly, 1992; Simmons and Kelly, 1989).  Combined effects  of
24      O3, rainfall acidity and soil Mg status on growth and ectomycorrhizal colonization of Pinus
25      taeda L has been studied (Simmons and Kelly, 1989). Although variation was high, there
26      was a trend towards altered species composition and reduced mycorrhizal infection in
27      O3 treated seedlings.  Edwards and Kelly (1992) found high variability in morphotype
28      (morphologically different) frequency in response to O3 treatments in P. taeda L., and noted
29      changes in morphotype frequency over the 3 year study that suggested fungal succession had
30      occurred.  Fungal succession and the effects of oxidant stress on normal successional patterns
       December 1993                          5.245      DRAFT-DO NOT QUOTE OR CITE

-------
 1     are poorly understood. Shaw et al. (1992), using an open field exposure system, found no
 2     differences in morphotype frequency or fruit-body succession in response to O3 treatments.
 3          In summary, there is evidence that O3 affects mycorrhizal symbioses in a number of
 4     plant species.  The mechanism appears to be through altered carbohydrate  allocation and
 5     availability in the root. Efforts are currently underway to address successional patterns of
 6     mycorrrhizal fungi under oxidant stress and should provide a more integrative understanding
 7     of the effects at the ecosystem level.
 8
 9     5.7.3.9  Rhizosphere and Soil Processes
10          The importance of the below-ground ecosystem has largely been overlooked when
11     evaluating ecological responses to oxidant exposure.  Although the soil system is part of the
12     larger terrestrial ecosystem, it is a system that operates independently and therefore is itself
13     an ecosystem (Richards, 1987). While above-ground components of the terrestrial ecosystem
14     are dominated by producers, the below-ground system is composed primarily of consumers.
15     Thus, the below-ground system is dependant on the above-ground system for inputs of
16     energy-containing substrates.  Bacteria, fungi, protozoa, nematodes, microarthropods,
17     earthworms and enchytraeids  all serve various functions in maintaining biological, physical
18     and chemical characteristics of soil, and all are dependent on plant residues for their
19     maintenance.  While the uniqueness of the below-ground ecosystem needs  to be recognized,
20     the interdependence between the above- and below-ground systems cannot  be over
21     emphasized.
22          Even though the effects  of O3 on rhizosphere and soil processes have not been studied,
23     potential impacts can be hypothesized based on known plant responses to O3.  As noted
24     above, O3 stress reduces photosynthesis and growth, and roots often are more affected than
25     shoots (Winner et al., 1991; McCool and Menge,  1984; Blum and Tingey, 1977; Manning
26     et al.,  1971; Tingey and Blum, 1973; Hogsett, 1985; Tingey et al., 1976;  Spence et al.,
27     1990; McLaughlin et al., 1982).  Oxidant stress has been shown to affect both leaf
28     senescence and root production in plants, thereby disnipting carbon availability for
29     maintenance of the below-ground system  (Gorissen et al., 1991; Andersen and Rygiewicz,
30      1991).
        December 1993                          5-246      DRAFT-DO NOT QUOTE OR CITE

-------
 1          The availability of current photosynthate for root growth appears to be reduced under
 2     O3 stress, and maintenance of below-ground processes dependent on roots for their carbon
 3     substrates may be affected.  As noted in the previous section, a 45% reduction in transport of
 4     photosynthates to roots occurred in O3 treated P. taeda (Spence et al., 1990).  Ozone reduces
 5     concentrations of root carbohydrates (Jensen, 1981; Tingey et al., 1976; Meier et al., 1990,
 6     Andersen et al., 1991).  Starch in roots was significantly reduced in P. ponderosa by the end
 7     of one growing season of O3 exposure (Tingey et al., 1976). Reductions in coarse and fine
 8     root starch concentrations persisted over the winter in O3-treated P. ponderosa and were
 9     lower during the subsequent years shoot flush (Andersen et al., 1991).  In this study, lower
10     starch concentrations in O3-treated seedlings were associated with suppressed growth of new
11     roots.  The consequences of a reduction in carbon  allocation below-ground includes reduced
12     substrate availability for soil flora and fauna, altered soil physical characteristics such as total
13     organic matter and aggregation, and altered soil chemical characteristics including cation
14     exchange capacity.
15          Premature leaf senescence has been observed in plants exposed to O3 stress (U.S.
16     Environmental Protection Agency, 1986).  Premature senescence affects the below-ground
17     ecosystem by reducing canopy photosynthesis and carbon availability for transport to the
18     below-ground system, and by increasing leaf litter inputs to the forest floor (Miller, 1982;
19     Fenn and Dunn,  1989).  The result is increased flux of nutrients,  especially N, below-ground
20     due to oxidant exposure.
21          The increased flux of nitrogen  due to premature needle senescence in oxidant exposed
22     plants may act to disrupt nutrient flow of the ecosystem. Allocation of carbon resources
23     throughout a plant is based on a priority scheme that is driven by carbon and nutrient
24     availability (Waring  and Schlesinger, 1985).  When soil nutrient levels are high, allocation to
25     the shoot is favored  over the roots.  By shifting carbon allocation to organs in this fashion,
26     plants can adjust to shifts in resource availability in their environment.  Oxidant  stress alters
27     typical allocation schemes and in the process may impair the plant's ability to cope with
28     drought or other stresses. In addition, reductions in allocation to  roots can alter root system
29     size, architecture and spatial arrangement, which in turn can influence populations of soil
30     organisms.
       December 1993                          5-247      DRAFT-DO NOT QUOTE OR CITE

-------
 1          Bacteria and fungi are particularly important in nutrient cycles and act to immobilize N,
 2     C, P, and other nutrients in their biomass.  The turnover of these nutrient pools are relatively
 3     short as bacterial and fungal preditors act to release these nutrients. The majority of plant
 4     available N during the growing season comes from these predatory interactions in the soil
 5     (Kuikman et al., 1991; Ingham et al., 1985), emphasizing their importance in the
 6     maintenance of terrestrial ecosystems.  Currently there are no data available on the effect of
 7     O3 on  soil  fauna.
 8
 9     5.7.4    Summary
10          Ecosystems are composed of populations of "self-supporting" and "self-maintaining"
11     living plants, animals and microorganisms (producers, consumers, and decomposers)
12     interacting with one another and with the nonliving chemical and physical environment within
13     which  they exist (Odum, 1989; U.S. Environmental Protection  Agency, 1993). Mature
14     ecosystems are seldom stable.  They must continually respond and adapt to changing
15     environments (Koslowski,  1985). Structurally complex communities, they are held in an
16     oscillating  steady state by the operation of a particular combination of biotic and abiotic
17     factors.
18          Ecosystem response to stress begins with  individuals.  Intense competition among plants
19     for light, water,  nutrients,  and space, along with recurrent natural climatic (temperature) and
20     biological  (herbivory, disease, pathogens) stresses, can alter the species composition of
21     communities by eliminating those individuals sensitive to specific stresses, a common
22     response in communities under stress (Woodell, 1970; Guderian, 1985).  Those organisms
23     able to cope with stresses survive and reproduce.  The effects of stresses upon ecosystems,
24     unless they are  catastrophic disturbances are frequently difficult to determine (Koslowski,
25      1985;  Garner et al., 1989)  In a mature forest, a mild disturbance becomes part of the
26     oscillating steady state of the forest community or ecosystem.  Responses to catastrophic
27      disturbances, however, as  a rule are readily observable and measurable (Garner, 1993).
28           Ecosystem responses are hierarchical ranging from those  that are characteristic of
29      individuals to those characteristic of the entire ecosystem.  Ecosystems integrate individual
30      responses  and propagate them through trophic and competitive relationships.  Two properties
31      that are important in determining the effect a stress at one hierarchial level of organization

        December 1993                          5-248      DRAFT-DO  NOT QUOTE OR CITE

-------
 1     will have on a higher level are variability and compensation.  Variability in response to stress
 2     may mean that, because of genetic variation, not all trees are equally susceptible.  At the
 3     stand level, the slower growth of some trees may be compensated for by the relatively faster
 4     growth of others that are experiencing reduced competition so that the overall growth of the
 5     stand is not affected  (Hinkley et al., 1992).  These properties when taken together will
 6     determine the extent  and rate at which stress at one hierarchical level will impact the next
 7     highest level.
 8          The mixed conifer forest ecosystem in the San Bernardino Mountains of southern
 9     California is one of the most thoroughly studied ecosystems in the United States.  The
10     changes observed in  the mixed conifer forest ecosystem exemplify those expected in a
11     severly disturbed ecosystem.  Chronic O3 exposures over a period of 50 or more years
12     caused major changes in the San Bernardino National Forest ecosystem.  The primary effect
13     was on the more susceptible members of the forest community, individuals of ponderosa and
14     Jeffrey pine, in that they were no longer able to compete effectively for essential nutrients,
15     water, light and space.  As a consequence of altered competitive conditions in the
16     community, there was a decline in the sensitive species, permitting the enhanced growth of
17     more tolerant species (Miller et al.,  1982; U.S. Environmental Protection Agency,  1978,
18     1986).  The results of the studies of the San Bernardino Forest ecosystem were reported in
19     both the 1978 and 1986 criteria documents (U.S Environmental Protection Agency,  1978,
20     1986).  The more recent data from the San Bernardino Forest and from other ecosystems in
21     California indicate that there continue to be 03 concentrations injurious to forest vegetation.
22     The concentrations and durations, however, are not as high nor for as long periods as in
23     former times.  For this reason, the vegetational injury has not been as great.
24          There is some indication from new data that O3 may not have been the only stress
25     encountered by the San Bernardino Forest ecosystem.  Nitrate deposition gradients similar to
26     those measured for O3 suggests the possible  soil-mediated exposures to nitrate could have
27     been anc continue to be combined with the foliage-mediated O3 exposures.  Research in this
28     area is continuing.
29          Studies of O3 induced vegetational injury in the Appalachian Mountains and the
30     southeastern United States is ongoing.  Preliminary results indicate that injury to sensitive
31     vegetation continues  to occur.

       December 1993                          5-249      DRAFT-DO NOT QUOTE OR CITE

-------
 1          Inhibition of photosynthesis by O3 exposure alters carbohydrate allocation from the
 2     shoot to the roots. Reduced carbohydrate allocation to the roots has been shown to affect
 3     mycorrhizae formation.  Mycorrhizae are extremely important for mineral nutrient uptake by
 4     trees and other vegetation reduction in their formation has been shown to have an detrimental
 5     impact on plant growth.
 6
 7
 8     5.8   EFFECTS OF OZONE ON  AGRICULTURE, FORESTRY, AND
 9           ECOSYSTEMS:  ECONOMICS
10     5.8.1   Introduction
11          Evidence from the plant science literature cited hi the  1986 O3 Criteria Document (U.S.
12     Environmental Protection Agency, 1986)  and in the present document is unambiguous with
13     respect to the  adverse effects of tropospheric O3 on some types of vegetation. For example,
14     findings from  U.S. EPA's multiyear NCLAN program provides rigorous corroboration of at
15     least a decade of previous research which showed that O3 at ambient levels caused physical
16     damage  to important species,  Specifically, NCLAN established that ambient O3 levels
17     resulted in statistically significant reductions in yields for these crops. Literature reviewed in
18     Section 5.6 of this document assesses the state of natural science findings regarding
19     O3 effects on  crops, forests and other types of vegetation in more detail.
20          Information on the benefits and costs of alternative policy options or states of the world
21     (such as changes in air pollution) is of use to decision makers in a variety of settings.  For
22     example, economic information provides one means by which to choose from alternative
23     policies  or public investments. The role of cost-benefit analysis in federal rule making or
24     standard setting was enhanced in  1981 by President Reagan's Executive Order 12291
25     (February 19, 1981) which  required that such calculations be performed on any  rule or
26     regulation promulgated by the federal government.  That executive order provided the
27     stimulus for a large increase in the use of economic analysis in evaluating federal actions,
28     including environmental policies. While the Clean  Air Act and its amendments  do not allow
29     the use of cost-benefit analysis in the standard setting process for primary (human health)
30     effects,  economic information has been introduced into the discussion of secondary or
       December 1993                         5-250     DRAFT-DO NOT QUOTE OR CITE

-------
  1      welfare effects. A number of economic studies addressing vegetation and other welfare
  2      effects have been performed  in the last decade.
  3           Assessments of the economic consequences of O3 on vegetation reflect the state of
  4      natural science information on each vegetation category.  The natural  science evidence
  5      concerning effects of O3 on individual tree species or plant communities is less secure than
  6      for agricultural crops (see  Section 5.6).  As a result, most economic assessments focus on
  7      agricultural crops.  The economics literature on effects of O3 and other air pollutants on
  8      forest productivity is very  sparse;  the few assessments are confined to evaluations of assumed
  9      or hypothetical changes in  output (e.g., board feet of lumber).  The economic effects of
10      O3 on plant communities or ecosystems have not been measured in any systematic fashion.
11           This section reviews  economic assessments across these vegetation categories.  The
12      discussion of economic valuation of ecosystem effects is limited to conceptual and
13      methodological issues in performing such assessments, given the absence of empirical
14      analyses in this category.
15
16      5.8.2   Agriculture
17           In view of the importance of U.S. agriculture to both domestic and world consumption
18      of food and fiber,  reductions in crop yields could adversely affect human welfare.  The
19      plausibility of this premise resulted in numerous attempts to assess, in monetary terms, the
20      losses from ambient O3 or the benefits of O3 control, to agriculture. Fourteen assessments
21      of the economic effects of  O3 on agriculture were reviewed in the  1986 document (U.S.
22      Environmental Protection Agency,  1986). Since the preparation of the 1986 document, there
23      have been at least nine other studies published in the peer review literature which provide
24      estimates  of the economic consequences of O3 on agriculture.
25           The 1986 document highlighted key issues in judging the validity of economic
26      assessments which are applicable to post-1986 studies (i.e., how well the biological,
27      aerometric, and economic inputs used in the assessment conform to specific  criteria).  First,
28      the evidence on crop response to O3 should reflect how crop yields will respond under actual
29      field conditions. Second, the air quality data used to frame current or hypothetical effects of
30      O3 on crops should represent actual exposures sustained by crops at individual sites or
31      production areas. Finally,  the assessment methodology into which  such data are entered

        December 1993                          5_25i      DRAFT-DO NOT QUOTE OR CITE

-------
 1     should (1) capture the economic behavior of producers and consumers as they adjust to
 2     changes in crop yields and prices that may accompany changes in O3 air quality; (2) should
 3     accurately reflect institutional considerations, such as regulatory programs and income
 4     support policies (e.g., provisions of federal "Farm Bill" legislation), that may result in
 5     market distortions; and (3) use measures of well-being that are consistent with principles of
 6     welfare economics.
 7
 8     5.8.2.1   Review of Key Studies from the  1986 Document
 9          Assessments  of O3 damages to agricultural  crops reported in the 1986 document
10     displayed a range of procedures for calculating economic losses, from simple monetary
11     calculation procedures to more complex assessment methodologies which conform to some or
12     all of the economic criteria above.  As noted in the 1986 document, the simple procedures
13     calculate monetary effects by multiplying predicted changes in yield or production resulting
14     from exposure to O3 by an assumed constant crop price. By failing to recognize possible
15     crop price changes arising from yield changes and not accounting for potential producer
16     responses, such assessments are flawed, except for highly restricted situations such as
17     localized pollutant events.  Conversely, some assessments provide estimates of the economic
18     consequences of O3 and other air pollutants that  reflect producer-consumer decision-making
19     processes, associated market adjustments, and some measure of distributional consequences
20     between affected parties.  The distinctions between studies based on naive or simple models
21     and those based on correct procedures is important at the regional or national level, since  the
22     simple procedures may be biased, leading to potentially incorrect policy decisions.
23          Most of the economic  assessments reviewed in the  1986 document (nine of the fourteen)
24     focused on O3 effects in  specific regions, primarily California and the Corn Belt (Illinois,
25     Indiana, Iowa,  Ohio, and Missouri).   There  have been a number of additional regional
26     assessments since the 1986 document; most are non-peer reviewed  reports  arising from
27     consulting or contract research.  This regional emphasis in the earlier literature may be
28     attributed to the relative abundance of data on crop response and air quality for selected
29     regions, as well as (he importance  of sonic agricultural regions, such as California,  in the
30     national agricultural economy.  Most  of the  recent state or regional assessments are
31     commissioned by state public utility commissioners or similar regulatory agencies and use

       December 1993                           5-252      DRAFT-DO NOT QUOTE OR CITE

-------
  1      variants of the simple "price times yield" approach, where yields are calculated from
  2      response functions arising from the NCLAN data.  While perhaps of use to Public Utility
  3      Commissioners concerned with effects from single power plants or other localized sources,
  4      these studies generally contribute little to the assessment of pollution effects at the national
  5      level.  (Most local or regional studies abstract  from physical and economic interdependencies
  6      between regions, which limits their utility in evaluating secondary national ambient air
  7      quality standards or NAAQS.)
  8           National-level studies which account for economic linkages between groups and regions
  9      can overcome some limitations of regional analyses.  A proper accounting of these linkages,
10      however, requires additional data and more complex models, and frequently poses more
11      difficult analytical problems. Thus, detailed national assessments tend to  be more costly  to
12      perform. As a result, there are fewer assessments of pollution effects at the national level
13      than at the regional level.
14           Two national studies reported in the 1986 document were judged to  be "adequate" in
15      terms of the three critical areas of data inputs.  Together, they provided a reasonably
16      comprehensive estimate of the economic consequences of changes in ambient air Qj levels on
17      agriculture.  Because of their central role in the 1986 document, these two studies are
18      reported in Table 5-33 and are  reviewed briefly below.
19           In  the  first of these studies,  Kopp et al. (cited as 1984 in the earlier document but
20      subsequently published as a journal article in 1985) measured the national economic effects
21      of changes in ambient O3 levels on the production of corn, soybeans, cotton, wheat,  and
22      peanuts. In addition to accounting for price effects on producers and consumers,  the
23      assessment methodology used is notable in that it placed emphasis on developing
24      producer-level responses to O3-induced yield changes (from NCLAN data available at the
25      tune) in 200 production regions.  The results of the Kopp et al.  study indicated that a
26      reduction in O3 from 1978 regional ambient levels to a seasonal 7-h average of
27      approximately 0.04 ppm would result in a $1.2 billion net benefit in 1978 dollars.
28      Conversely, an increase in O3 to an assumed ambient concentration of 0.08 ppm (seasonal
29      7-h average) across all regions produced a net  loss of approximately  $3.0  billion.
30          The second study, by Adams et al. (originally cited as 1984b, but subsequently
31      published as a journal article in 1986a), was a  component of the NCLAN  program. The

        December 1993                           5.253      DRAFT-DO NOT QUOTE OR CITE

-------
                 TABLE 5-33. RECENT STUDIES OF THE ECONOMIC EFFECTS OF OZONE AND
                                    OTHER POLLUTANTS ON AGRICULTURE3
a
sr
i
i—*
\o
VO
u>














LA
hJ
Ul
•^

U
C
2
i
O
O
2!

/-)
e
^-<
S
i

Model Features
Pollutant and Price Output Input Quality
Region Concentration Changes Substitutions Substitutions Changes
Illinois Ozone. 10% increase No Yes Yes No
from 46.5 ppb
U.S. Ozone. 25% reduction Yes Yes Yes No
from 1980 level for each
slate
U.S. Ozone, universal Yes Yes Yes No
reduction from 53 ppb to
40ppbb
U.S. Ozone, universal Yes No No Yes
reduction from 53 ppb to
49 ppba
U S Acid deposition, 50% Yeh Yes Yes No
reduction in wet acidic
deposition
U.S Ozone. 10% reduction Yes Yes Yes No
from annual levels
(1986- 1990) for rural
areas. Includes
adjustments for 1985
Farm Bill.
U.S. Ozone, seasonal standard Yes Yes Yes No
of 50 ppb with 95%
compliance ; includes
adjustments for 1985
Farm Bill.
U.S. Increased UV-B radiation Yes Yes Yes No
and associated increase
of tropospheric pj (of
16%)

"All studies except Garcia et al. use NCLAN data to generate yield changes due to ozone.
Seven-hour growing season geometric mean. Given a log-normal distribution of air pollution events,
not to be exceeded more than once a year Heck et al. (1982).



Crops
Corn, soybeans

Corn, soybeans,
cotton, wheat,
sorghum, barley
Corn, soybean,
wheat, cotton,
peanuts
Soybeans


Soybeans


Corn, cotton,
soybeans, wheat




Corn, soybeans,
cotton, wheat,
sorghum, rice, hay,
barley

Soybeans (for
UV-B) and all
crops in Adams
et al. (1989) for
tropospheric 03

Results (Annual 1980 U.S. Dollars)

Consumer Producer Total Benefits
Benefits Benefits (Costs)
None $226 x 10° $226 x 106

$1.160 x 106 $550 x 106 $1,700 x 106


Not reported Not reported $1,300 x 106


$880 x 106 $-90 x 106 $790 x 106


$172 x 106 $-30 x 106 $142 x 106


NA NA $2,500 x 106
(sum of
discounted
values at 5 % ,
1986-1990)

$905 x 106 $769 x 106 $1,674 x 106




NA NA -830 x 106 (for
the increase in
tropospheric Qj
only)





Study
Garcia et al.
(1986)
Adams et al.
(1986)d

Kopp et al.
(1985)d

Shortle et al.
(1986)

Adams et al.
(1986)

Kopp and
Krupnick (1987)




Adams et al.
(1989)



Adams and Rowe
(1990)




a 7-h seasonal ozone level of 40 ppb is approximately equal to an hourly standard of 80 ppb,
cSevenand 12-h growing season geometric mean. Analysis includes both fixed roll-backs (e.g., 25%) and seasonal standards (with variable compliance rates).
Tteported in 1986 Criteria Document.

-------
 1     results were derived from an economic model of the U.S. agricultural sector that includes
 2     individual farm models for 63  production regions integrated with national supply and demand
 3     relationships for a range of crop and livestock activities. Using NCLAN data, the analysis
 4     examined yield changes for six major crops (corn, soybeans, wheat, cotton, grain, sorghum,
 5     and barley) that together account for over 75 % of U.S. crop acreage. The estimated annual
 6     benefits (in 1980 dollars) from O3 adjustments are substantial, but make up a relatively small
 7     percentage of total agricultural output (about 4%).  Specifically, in this  analysis, a 25%
 8     reduction in O3 from 1980 ambient  levels resulted in benefits of $1.7 billion.  A 25%
 9     increase in O3 resulted in an annual loss (negative benefit) of $2.4 billion. When adjusted
10     for differences  in years and  crop coverages, these estimates are  close to the Kopp et al.
11     (1986a) benefit estimates.
12           The Kopp et al. (1985) and Adams et al. (1986a) studies indicated that ambient levels
13     of O3 were imposing substantial economic costs on agriculture.  However, both Kopp et al.
14     (1985) and Adams et al.  (1986a) were judged to suffer from several sources of uncertainty.
15     These include the issue of exposure dynamics (7-h per day exposures from the NCLAN
16     experiments versus longer exposure periods, such as  12-h exposures), and the lack of
17     environmental interactions, particularly O3-moisture stress interactions,  in many of the
18     response experiments. Also, the O3 data in both studies are based on a limited set of the
19     monitoring sites in the AIRS system, mainly sites in urban and suburban areas.  While the
20     spatial interpolation process used for obtaining O3 concentration data (Kriging) resulted in a
21     fairly close correspondence between predicted and actual O3 levels at selected validation
22     points, validation for rural sites was limited (Lefohn et al.,  1987).  The economic models,
23     with  their large number of variables, and parameters,  and the underlying data used to derive
24     these values, were also noted as potential sources of uncertainty, including the effects on
25     economic estimates of market-distorting factors such as the federal farm programs.  Concern
26     over  farm programs stems from the evidence that reductions in O3 will  increase yields and
27     hence total production of some crops.  If the crop is covered (eligible for deficiency
28     payments) under the provisions of the farm program, then the total costs to the government
29     (of the farm program) may increase as  a  result of reduced  O3 (McGartland, 1987).  Thus,
30     the benefits of the O3 reduction may not be as great as estimated.
       December 1993                          5.255      DRAFT-DO NOT QUOTE OR CITE

-------
 1          The 1986 criteria document concluded that these possible improvements in future
 2     assessments were not likely to alter greatly the range of agricultural benefit estimates for
 3     several reasons. First, the studies covered about 75 to 80% of U.S. agricultural crops (by
 4     value). For inclusion of the other 20% to change the estimates significantly would require
 5     that their sensitivities to O3 be much greater than for the crops included to date.  Second,
 6     model sensitivity analyses reported in past studies indicate that changes in plant exposure
 7     response relationships must be substantial to translate into major changes in economic
 8     estimates.  For example, it was believed unlikely that use of different exposure measures or
 9     inclusion of interaction effects would greatly alter the magnitude of the economic estimates.
10     Third, it was believed that there were likely to be countervailing effects that would mitigate
11     against large swings in the estimates (e.g., longer exposure periods may predict greater yield
12     losses), but O3-water stress tends to dampen or reduce the yield estimates.  Finally,  the
13     document noted that potential improvements in economic estimates are policy-relevant only to
14     the extent that they alter the relationship between total benefits and total costs of that policy.
15     The possible exception to this generally optimistic assessment of the robustness of the
16     estimates was inclusion of market-distorting factors (i.e., farm programs), an issue which is
17     addressed in some of the post-1986 assessments reviewed below.
18
19     5.8.2.2   A Review of Post-1986 Assessments
20           The 1986 document concluded that the O3 assessments by Kopp et al. (1985) and
21     Adams et al. (1986a) provided the most defensible evidence in the literature at that time of
22     the general magnitude of such effects.  These two studies, in combination with the
23     underlying NCLAN data on yield effects,  were judged to be the most comprehensive
24     information available on which to evaluate the economic impact of ambient air quality (O3)
25     on crops.
26           Seven national-level assessments performed since the last criteria  document are reported
27     in Table 5-33.   Of these, all use defensible economic approaches to quantify dollar effects,
28     where "defensible" is measured in terms of conforming to the criteria cited earlier.
29     An evaluation of these  studies in terms of the adequacy of critical plant science, aerometric,
30     and economic data is presented  in the table, along with estimates of benefits or damages
31     associated with changes in O3.

       December 1993                          5-256      DRAFT-DO NOT QUOTE OR CITE

-------
  1           The concluding statements in the 1986 document are a benchwork against which to
  2      judge these seven national level studies published since the last document.  Most of the
  3      contemporary studies build on either Kopp et al. (1985) or Adams et al.  (1986a); indeed, the
  4      motivation of some of the more recent studies is to test whether the problems noted above
  5      (such as exclusion of farm programs) are sufficient to alter the original estimates in a
  6      meaningful manner.  A relevant question is whether these new studies provided any
  7      "surprises"  in terms of magnitude of economic effects.   These studies are summarized in
  8      Table 5-33.
  9           In discussing these latest evaluations, there are several points which relate to their
10      comparability with Kopp et al.  (1985) and Adams et al.  (1986a).  First, all studies use
11      NCLAN response data to generate yield effects (for inclusion in the respective economic
12      models).  In most cases, data used in the post-1986 assessments reflect improvements of
13      earlier NCLAN data.  Second,  these studies may be characterized as second generation
14      assessments.  They build on the first generation of studies reported in the 1986 document by
15      refining selected aspects of those earlier studies, including (1) interactions with other
16      stresses; (2) use of aerometric data and assumptions which, in some cases, more closely
17      follow the seasonal and regional characteristics of O3 exposure (Adams et al., 1989);  and
18      (3) effects of O3 on quality of commodities (Shortle et al., 1986). Several of the studies use
19      updated versions of the economic models in Adams et al. (1986a) and Kopp et al. (1985).
20      In addition, some of the studies model the effects of government programs to judge the
21      potential consequences of such  distortions on economic  estimates (Kopp and Krupnik, 1987;
22      Adams  et al., 1989).  Third, there are differences in underlying aerometric assumptions;
23      some studies include both O3 and other environmental stresses (e.g., acid deposition,  UV-B
24      radiation); others reflect O3 data for more recent time periods. Since ambient O3 levels vary
25      across years, the choice of year will influence the yield estimates and ultimately the
26      economic estimates.
27           Common themes or findings from these (and earlier) O3 and other air pollution studies
28      have been summarized in two recent  synthesis  papers (Adams and Crocker, 1989; Segerson,
29      1991).  The results of the post-1986 assessments in Table 5-33 and the recent synthesis
30      papers corroborate the general findings of the 1986 document.  Specifically, the agricultural
31      effects of tropospheric O3 at ambient levels impose economic costs to society (or conversely,

        December 1993                           5.257      DRAFT-DO NOT QUOTE OR CITE

-------
 1     that reductions in ambient O3 result in societal benefits).  The magnitude of the economic
 2     costs reported in the more recent studies is similar to the estimates in Kopp et al. (1985) and
 3     Adams et al. (1986a).  Such a similarity is not surprising, given the points noted above
 4     concerning use of similar data and economic models.
 5          One important recent finding pertains to farm program. In each case, the inclusion of
 6     farm programs in the economic models resulted in modest changes (reductions) in the
 7     economic benefits of O3 control (due to increased farm program costs).  As Segerson notes,
 8     however, it is not clear that these increased costs should be charged against the potential
 9     benefits of an O3 regulatory  standard but rather as an additional cost associated with the
10     inefficiencies of the federal farm program.  Even with the inclusion of farm programs and
11     other elements the general magnitude of further effects reported in the 1986 document are
12     only reduced by approximately 20%.
13          In addition to including farm programs, there are a  couple of other notable additions to
14     the assessment literature.  One study (Adams et al., 1989) attempts to analyze economic
15     benefits under a regulatory alternative involving a  seasonal (crop growing season)
16     O3 exposure index measured as a 12 h mean, instead of hourly  levels or percent changes
17     from ambient reported  in earlier studies.  Specifically, a seasonal  average of 50 ppb
18     O3 (measured as a 12-h seasonal average) with a 95% compliance level, is reported in
19     Adams et al. (1989). The result (of a $1.7 billion benefit) is similar to the assumed 25%
20     reduction across all regions reported by Adams et  al. in 1986a.  At least one study has also
21     combined environmental stresses (e.g., O3, UV-B, radiation) in preforming economic
22     assessments. Adams and Rowe (1990), using the same model as Adams et al.  (1986a,
23     1989), report that a 15% depletion of stratospheric O3 (which results in a 13% increase in
24     tropospheric O3)  caused an economic loss of approximately $0.8 billion attributed to the
25     tropospheric O3  increase.
26
27     5.8.2.3   Limitations  and Future Research Issues
28          The recent literature (post-1986) on economic effects of O3 on agriculture supports the
29     general conclusions drawn in the 1986 document.  That is, ambient levels of O3 are imposing
30     economic costs on producers and consumers.  However,  there are at least three issues which
31     are not addressed in the extant literature on the topic.  First, the existing assessments do not

       December 1993                          5-258      DRAFT-DO NOT QUOTE OR CITE

-------
 1     consider the external costs of changes in agricultural production arising from changes in
 2     O3 exposures (Sergerson, 1990).  These costs are important if changes in O3 result in
 3     changes in crop mixes or production practices, which in turn result in changes in soil
 4     erosion, fertilizer and pesticide runoff or other agricultural externalities. For example, if
 5     reductions in O3 increase the relative profitability of a crop which uses higher levels  of
 6     chemical inputs, then some increase in chemical effluent may result.  Given that some
 7     assessments suggest that such changes in crop mixes and production practices  are likely to
 8     accompany O3 changes, these costs/benefits need to be addressed.
 9           A second issue not directly assessed in the current literature is the relationship between
10     climate change and tropospheric  O3 effects.  This relationship is important if global warming
11     is expected to increase tropospheric O3 levels. In addition, research  indicates that global
12     climate change will  lead to a relocation of crops  (Adams et al., 1990). This relocation may
13     change the vulnerability of crop  species to O3, given the spatial distribution of O3 across the
14     U.S. (i.e., increased crop production in areas of relatively low ambient O3, such as the
15     Pacific Northwest, implies lower O3 damage).
16           A third issue involves the institutional setting in which agricultural production occurs.
17     Several recent studies have assessed O3 effects in the presence of federal farm programs.
18     However, the U.S. and most industrialized economies are moving away from price supports,
19     production quotas and import restrictions,  the traditional form of government intervention  in
20     agriculture.  At the  same time that these market distortions are being removed,  there is
21     increasing government regulation of agricultural production practices to reduce  agricultural
22     externalities.  Future assessments of O3 effects may need to pay less  attention to farm
23     program effects and instead include other institutional features of U.S. Agriculture.
24
25     5.8.3   Forests (Tree Species)
26           The plant science literature on O3 and other air pollutant effects on tree species is
27     evolving rapidly as a result of recent research initiatives by EPA and other agencies.   The
28     long-term nature of  air pollution effects of perennial species creates challenges to plant
29     scientists in sorting out the specific effects of individual stresses  from among the many
30     potential explanatory factors, such as O3 (Skelly,  1989).  It also creates problems in terms of
        December 1993                           5-259      DRAFT-DO NOT QUOTE OR CITE

-------
 1     measuring impacts of direct economic value, such as reductions in board-feet of lumber
 2     produced per unit of time.
 3          To date, most natural science literature on forest species reports O3 effects in terms of
 4     foliar injury or similar measures (Taylor and Hanson,  1992; Davis and Skelly, 1992; Simini
 5     et al.,  1992; Freer-Smith and Taylor,  1992).  This emphasis on foliar effects (rather than
 6     marketable yield) is similar to the state of science for agricultural crops prior to 1975. Such
 7     visible foliar effects information is of limited use in economic assessments .  The exception
 8     is in measuring the economic value of aesthetic changes in a forest stock (see Crocker,
 9     1985a).
10          The lack of usable data concerning changes in marketed output, such as board-feet  of
11     lumber (or even changes in growth rates), has limited the number of economic assessment of
12     O3 effects on forests.  The few  studies which attempt to measure economic losses arising
13     from O3 or other pollutants circumvent the lack of plant science data by assuming (arbitrary)
14     reductions in forest species growth or  harvest rates (Callaway et al., 1985; Haynes and
15     Adams,  1992 ; Adams,  1986; Crocker and Forster, 1985).
16          These studies are summarized in Table 5-34. While the economic estimates reported in
17     Table 5-34 are comparable to these reported for agricultural crops (e.g., $1.5 billion for
18     eastern Canada, $1.7 billion for eastern U.S. forests),  the lack of defensible natural science
19     data makes these studies suggestive at best,  of possible economic consequences of forest (tree
20     species effects) of O3 or other environmental stresses.  In addition,  the economic
21     methodology used  in the assessments varies, from simple price times quantity calculations
22     (e.g., Crocker, 1985b) to the use of large, econometric-based  representations of the U.S.
23     timber market (Haynes and Adams, 1992).  With appropriate data,  the TAMM methodology
24     laid out by Haynes and Adams  holds promise for assessing the economic consequences of
25     O3 when requisite natural science data become available.
26          In  summary, the plant science literature shows that O3 adversely influences the
27     physiological performance of tree species; the limited economic  literature also demonstrates
28     that changes in growth have economic consequences.  However, the natural science and
29     economic literature on the topic is not yet mature enough to conclude unambiguously that
30     ambient O3 is imposing economic costs. The output from on-going natural science research
        December 1993                          5-260      DRAFT-DO NOT QUOTE OR CITE

-------
      TABLE 5-34.  STUDIES OF THE ECONOMIC EFFECTS OF OZONE AND
                          OTHER POLLUTANTS ON FORESTS



Pollutant/Coverage
All pollutants. Forest
products (hardwood
and softwood) in the
eastern U.S.




Acid deposition.
Forest products and
forest ecosystem
service flows for
eastern U.S.




Response and Air
Quality Data
Assumes three
arbitrary growth
reductions (10%,
15% and 20%) for
hardwood and
softwood tree
species.

Assumes a 5%
reduction in products
due to acid
deposition: assumes
a pristine background
pH of approximately
5.2



Economic Model
Spatial equilibrium
models of
softwood and
hardwood
stumpage and
forest products
industries in the
U.S.
Naive; assumed
changes in output
multiplied by
average value of
those goods or
services.

Annual
Damages or
Benefits of
Control
($ billion)
-270 X 106 to
563 X 106
damage in 1984
dollars for
assumed
reductions in
growth levels

-1,750 X 106
damage in 1978
dollars from
current levels of
acid deposition





Study
Callaway et al.
(1985)






Crocker (1985b)






 Acid deposition.
 Forest products and
 forest ecosystem
 services for eastern
 Canada.
 Air pollutants.
 including acid
 precipitation.  Losses
 estimated for eastern
 U.S softwoods.
Assumes 5%
reduction in forest
productivity for all
eastern Canadian
forests receiving
> 10 kg/ha/year
sulphate deposition.

None; paper
demonstrates a
methodology for
assessing economic
effects of yield
(growth and
inventory) reductions
due to any course.
Assumes losses  from
6 to 21 % for
softwoods.
Naive; assumed
changes in output
multiplied by
average value of
goods or services.
Econometric model
of U.S. timber
sector (TAMM).
-1,500 X 10°      Crocker and
damage in 1981    Forster (1985)
Canadian dollars
from current
levels of acid
deposition
-1,500 x
-7,200 X
1986 dollars
106to
106in
Haynes and
Adams (1992)
December 1993
                     5-261
             DRAFT-DO NOT QUOTE OR CITE

-------
 1     on this topic will be important to our understanding of this potentially important class of
 2     effects.
 3
 4     5.8.4   Valuing Ecosystem Service Flows
 5     5.8.4.1   Background
 6          Over the last thirty years economists have developed a variety of techniques for
 7     assessing the value of nonmarket goods and services [recently surveyed by Braden and
 8     Kolstad (1991) and Smith (1993)].   "Nonmarket" refers to those goods and services not
 9     priced and traded in markets.  While most applications are to natural resources and
10     environmental assets, the concepts  extend to a range of goods not usually traded in markets.
11     Early applications focused primarily on commodities used directly by the consumer,  such as
12     outdoor recreation.  Within the last decade, attention has  shifted to estimating nonuse
13     (or passive) values, such as what individuals are willing to pay to insure the existence of
14     species or unique natural settings.  The values elicited with these techniques are being used
15     in an increasing  array of settings; however, their use is not without controversy.
16          Valuing complex ecological functions and the associated range of ecosystem service
17     flows is relatively uncharted territory and raises a number of conceptual and practical issues.
18     Some difficulties in valuing ecosystem services lie in the  inability of ecologists to
19     unambiguously define and measure ecosystem  performance  and endpoints (see Section 5.7  of
20     this chapter).  Other problems arise from the inability of  economic science to measure
21     adequately the consequences of long-term and  complex phenomenon. A related problem is
22     the difference in disciplinary perspectives between ecologists and economists. As a result,
23     the current state-of-the-art for valuing ecosystem service flows is inadequate for benefit-cost
24     assessments used in environmental regulatory processes.  As Costanza et al.  (1991) state:
25            Because  of inherent difficulties and uncertainties in determining values,
26            ecological economics acknowledges several  different independent approaches.
27            There is  no consensus on which approach is right  or wrong — they all tell us
28            something — but there is agreement that better valuation of ecosystem services
29            is an important goal for ecological economics.  [Bold emphasis added]
30
31     Improvement in valuation of ecosystem service flows  will require increased interdisciplinary
32     cooperation and research between  ecologists and economists, including the development of a
33     shared language.  The objectives of this section are to provide a brief background on

       December 1993                          5-262      DRAFT-DO NOT QUOTE OR CITE

-------
 1     nonmarket valuation techniques, outline some of the conceptual issues which require
 2     resolution, and to offer an agenda for future research.
 3
 4     5.8.4.2   The Economic Perspective
 5           Economic analysis is one input to the full social accounting of environmental planning
 6     and management.  For example, Tingey et al. (1990) discuss a variety of viewpoints for
 7     defining "adverse effects" from ambient air quality, with economics being just one
 8     perspective.  More specifically, economic values are only one type of assigned values
 9     (Brown, 1984).  They reflect human preferences for a good or service,  and are not inherent
10     in the good or service itself.  Further, economic values are exchange values; they reflect the
11     terms of trade—dollars for services.  Decision criteria which are based on economic values,
12     such  as efficiency and benefit-cost analysis (BCA), reflect a particular utilitarian
13     philosophical perspective. Such a perspective is typically based on the notions of
14     "welfarism" (only  individual assessments of value count), and "consequentialism"
15     (assessment of value is based on identified outcomes or consequences) (Sen, 1987). While
16     economists do not deny the existence or validity of alternative perspectives of value, they do
17     assert the importance of economic values in making some types of private and social choices.
18           For example, terms such as "ecosystem management" are likely to reflect a broad
19     spectrum  of choices for policy makers.  Each choice may imply an alternative path for
20     attaining a given "state" of biological diversity or ecological health.  Each state will, in turn,
21     imply a different mix of endpoints (or outputs). Ecosystem management will alter the mix of
22     goods and services provided by a natural system,  requiring tradeoffs between these
23     endpoints. Accurate assessment of these tradeoffs in selecting the optimal path and
24     subsequent endpoints poses numerous challenges.  Economists believe that economic values
25     can aid in making  such difficult social choices.
26           A critical first step in applying economy reasoning is the distinction between  different
27     economic value components.  The most familiar component involves market values.  Market
28     values (prices) convey incentive information that guides the numerous independent decisions
29     that directly affect ecosystems (Perrings et al., 1992). However, market values typically will
30     not reflect the full  social welfare change that results from a change in ecosystem service
       December 1993                          5-263      DRAFT-DO NOT QUOTE OR CITE

-------
 1     flows. The distinction between market values and total social valuation requires the
 2     introduction of nonmarket values and the notion of total economic value.

 3           One taxonomy of economic values can be given as follows:
 4
 5            (1)  Direct use values (DUV):  determined by the contribution of an
 6                environmental asset to current production or consumption (e.g., timber
 7                harvest, recreation).
 8
 9            (2)  Indirect use values (IUV):  determined by the functional service flows
10                from the environment which support current and future production and
11                consumption (e.g., watershed protection, natural filtration of polluted
12                water, ecological functions).
13
14            (3)  Option value (OV): refers to the value individuals place on the potential
15                future use of a resource (willingness to pay today  for option to exercise
16                future use of an  environmental asset).
17
18            (4)  Bequest value  (BV): refers to the present generation's preference for
19                bequest to future generations.
20
21            (5)  Existence value  (EV):  contemplative values for the existence of a
22                resource  arising  independent of any current or future in situ use of the
23                resource).
24
25
26           A number of similar value taxonomies exist (e.g., Munasinghe, 1992; Pearce, 1993).

27     The critical distinction for decision-making is between goods and services whose economic
28     values are or are not fully captured in  market prices.  For example, timber products may
29     have a direct use value which is accurately  reflected by market prices.  Recreation may also
30     have a direct use value, but minimal or nonexistent fees do not accurately reflect this value.
31     Nonuse values, by definition, have no discernible link to market behavior. Specialized

32     techniques must be used to assess these values in a manner commensurate with more
33     conventional commodities (e.g., timber production sold in a market).  Of the class of
34     nonmarket goods and services, the critical distinction is between use values and nonuse

35     values.
36           The measurement of total economic value (TEV) refers  to systematic attempts to assess

37     the combined economic values of an environmental asset or resource system (Pearce, 1993;
38     Peterson and Sorg, 1987; Randall, 1991b). In the same way that physical resource functions

39     are interconnected, economic values for the various goods and services produced are

       December 1993                          5-264      DRAFT-DO NOT QUOTE OR CITE

-------
  1     interconnected. A valid TEV measurement must account for this interconnectedness (e.g.,
  2     substitution and complementarity issues, and non-additivity of component parts).  While the
  3     concept of TEV is generally accepted by economists, systematic attempts to measure TEV in
  4     a regional policy or planning context are rare.
  5
  6     5.8.4.3  Nonmarket Valuation: Implications for Ecosystem Service Flows
  7          Nonmarket valuation techniques consist of two basic types.  Indirect approaches rely on
  8     observed behavior to infer values. Direct approaches use a variety of survey-based
  9     techniques to directly elicit preferences for nonmarket goods and services. Both sets of
 10     techniques share a common foundation in welfare economics, where measures of willingness-
 11     to-pay  (WTP) and willingness-to-accept (WTA) compensation are taken as the basic data for
 12     individual benefits and costs.
 13
 14     Indirect Approaches
 15          Indirect approaches, sometimes referred to as revealed preference  approaches, rely on
 16     observed behavior to infer values. Examples include the travel cost method (TCM) where
 17     the relationship between visits and travel expenditures is used to infer the value of a
 18     recreational site, and hedonic pricing method (HPM) which attempt to decompose the value
 19     of market goods, say recreational real estate adjacent to a national forest, to extract the
 20     embedded values for environmental assets.  Travel  cost methods encompasses a variety of
 21      models ranging from the simple single site travel cost model, to regional and generalized
 22      models which incorporate quality indices and account for substitution across sites.  Hedonic
 23      pricing method encompasses both land price and wage models which account for variations
 24      due to environmental attributes (e.g., air and water quality, noise, aesthetics, environmental
 25      hazards). The indirect approaches can only measure use values.  This limitation is brought
 26      out in one fairly strong assumption (weak complimentarity) which requires that associated
 27      with consumption of an environmental good  or service is the purchase of some market good,
 28      and when consumption of the market good is zero then demand for the environmental good
29      or service is almost zero (Adamowicz, 1991).  Recent summaries of the indirect approaches
30      can be found in Braden and Kolstad (1991), Mendelsohn and Markstrom (1988), Peterson
31      et al.  (1992) and Smith (1989, 1993).

        December 1993                          5_265     DRAFT-DO NOT QUOTE OR CITE

-------
 1          A brief hypothetical example illustrates the use of an indirect approach to measuring
 2     nonmarket value. The HPM can be applied to housing prices to estimate the value of
 3     environmental attributes, such as "clean air" or proximity to wetlands, which vary across a
 4     region.  It is assumed that variations in housing prices can be linked to real or perceived
 5     variations in these environmental attributes, (controlling for a variety of other statistical
 6     determinants).  In practice, the approach involves collection of cross sectional data on house
 7     sales (or possibly assessed values) and information on a menu of potential determinants of
 8     value (lot size, number of bedrooms, etc.). These factors would include one or more indices
 9     of environmental attributes or services. Through multivariate statistical techniques, the
10     marginal value of either positive or negative environmental externalities can be inferred. For
11     example,  it might be found that the average homeowner in a particular county would pay
12     $X to be Y  meters closer to an open-water wetland, and would require a reduction in price
13     of $Z to be  Y meters closer to a smoke-producing factory.
14          Applications of HPM are limited to use values and work best where  there is some
15     identifiable spatial distribution of value.  Continued improvements in available natural
16     science information (e.g.,  geographic information systems—GIS) will improve the efficacy
17     and precision of future HPM  applications to environmental services. While direct  use of
18     GIS-based information is rare in HPM models  (Doss and Taff,  1993), this is a likely area of
19     future research expansion.
20
21     Direct Approaches
22          Direct approaches to nonmarket valuation are survey-based techniques to directly elicit
23     preferences.  The hypothetical nature of these experiments requires that markets  (private
24     goods or political) be "constructed" to convey  a set of changes to be valued. While there are
25     a number of variants  on these constructed markets, the most common is the contingent
26     valuation method (CVM).
27           Contingent valuation method can be  viewed as a highly structured conversation (Smith,
28      1993) which provides respondents with background  information concerning the available
29     choices and specific increments or decrements in one or more environmental goods.  Values
30     are elicited  directly in the form of statements of maximum WTP or minimum WTA
31     compensation for the hypothetical changes in environmental goods.  For example,

        December 1993                          5-266       DRAFT-DO NOT QUOTE OR CITE

-------
 1      recreational anglers may be asked about their WTP for specific increments in run size for a
 2      fishery (Johnson and Adams, 1989). Typically, multivariate statistical techniques are used to
 3      model a WTP function.  Such models allow the analyst to control for variation in the
 4      personal characteristics of the respondents, check  for consistency of results with economic
 5      theory, and possibly estimate an entire WTP response surface across varying levels of
 6      environmental goods.
 7           The contingent valuation method can be applied to both use and nonuse values.  The
 8      flexibility of constructing hypothetical markets accounts for much of the popularity of the
 9      technique.  There are numerous methodological issues associated with application of CVM
10      including how the hypothetical environmental change is to be specified, the elicitation format
11      for asking valuation questions, the appropriate welfare measure to be elicited (i.e., WTP or
12      WTA), and various types of response biases.  Randall (1991a) argues that because of the
13      importance of nonuse values, CVM is likely to be the primary tool for measuring the
14      environmental benefits of biodiversity.  Recent summaries of CVM can be found in Mitchell
15      and Carson (1989) and Carson (1991).
16
17      Nonuse Values
18           From a measurement  perspective, "passive"  or nonuse values (i.e., option, existence
19      and bequest) are the most problematic component of TEV.  The contingent valuation method
20      is the only technique available for assessing these  values.  The topic of existence values for
21      environmental assets is one of the most controversial  in environmental economics (Bishop
22      and Welsh, 1992; Edwards, 1992;  Kopp, 1992; Rosenthal and Nelson, 1992).  Evidence
23      shows that individuals will  contribute to environmental organizations, and express positive
24      WTP to preserve environmental assets on CVM surveys,  with no expectation of current
25      period or future use of the  resource. However, evidence that existence values "exist" is
26      something less than arguing that they can be measured on a sufficiently comprehensive and
27      reliable basis for use in formal decision rules (Castle  and Berrens, 1993; Rosenthal and
28      Nelson,  1992).
29           An example of some of the ambiguities in existence value estimation can be seem in a
30      CVM study by  Stevens et al. (1991a) on bald eagles,  wild turkeys, and Atlantic Salmon in
31      New England.  While Stevens et al. (1991a) found substantial economic benefit from

        December  1993                           5_267      DRAFT-DO NOT QUOTE OR CITE

-------
 1     protection and restoration programs, their results also indicate that in a setting of potential
 2     irreversibiiity, existence values were difficult to quantify and sensitive to how the species
 3     were aggregated. Further,  a majority of respondents viewed species protection as important,
 4     but were unwilling to pay anything. Follow-up questions indicated that many respondents
 5     were uncertain of their values or protested the WTP question for ethical reasons.
 6          Much of the controversy over nonuse values has been stimulated by debates
 7     surrounding natural resource damage assessment and liability cases (e.g., the Exxon Valdez
 8     oil spill in Alaska). This controversy among economists is highlighted by the recent blue-
 9     ribbon panel, containing several Nobel Laureate economists, convened by  the U.S.
10     Department of Commerce's National  Oceanic and Atmospheric Administration (NOAA) in
11     1992.  The panel was convened to provide guidance concerning the potential use of CVM in
12     measuring lost passive or nonuse values  in promulgating regulations, pursuant to the Oil
13     Pollution Control Act of 1990.  The potential for assessing nonuse values through application
14     of CVM was essentially reaffirmed by the NOAA panel, provided rigorous guidelines are
15     followed (Arrow et al., 1993).
16           There are a variety of recent examples of the application of CVM to measure existence
17     values,  including Columbia River salmon (Olsen et al.,  1991), and forest protection (Hagen
18     et al.,  1992; Loomis et al., 1993; Rubin et al., 1991).  Some economists remain skeptical
19     that  existence values can be reliably measured for endangered species  and  irreversibiiity
20     problems (Castle and Berrens,  1993;  Stevens et al.,  1991b), and turn from the traditional
21     benefit-cost framework towards more ecologically conservative decision criteria such as the
22     safe minimum standard (SMS) of conservation  (Ciriacy-Wantrup, 1952).
23
24     Use Values
25           Empirical estimates of nonmarket  use values are less controversial, and are important
26     inputs to some types of research planning processes.  The extant literature contains hundreds
27     of site-specific studies valuing recreational services and environmental quality.  Recent
28     examples involving natural  resources include Donnelly et al.  (1990), Duffield et al.  (1992),
29     Johnson and Adams (1989), Morey et al. (1991).  Viewed  in the aggregate, the numerous
30     valuation studies document the considerable economic worth of nonmarket goods and
31     services.

       December 1993                          5-268      DRAFT-DO NOT QUOTE OR CITE

-------
  1           An emerging issue in the valuation literature is the need to develop acceptable
  2      procedures for transferring values (Brookshire and Neil, 1992; Walsh et al., 1992).  Benefit
  3      transfer refers to the transfer of some existing valuation estimate (or function) from the study
  4      site to a policy site.  For example, incorporation of "typical" nonmarket values for
  5      recreation, fish and wildlife occurs in the U.S. Forest Service planning process under the
  6      Resource Planning Act (RPA) of 1974,  as amended (Duffield,  1989).  It should be noted,
  7      however, that these "RPA values" differ greatly from state-of-the-art primary data studies
  8      (Olsen, 1989), perhaps because the RPA values do not incorporate nonuse values (Duffield,
  9      1989).
10
11      5.8.4.4   Challenges in Linking Valuation Techniques to Ecosystem Service Flows
12           The need for and  interest in values of nonmarket goods and services has arisen
13      independently of concerns regarding  ecosystem management and sustainability.
14      As environmental planning and management change to accommodate new issues, the need for
15      de novo valuation studies may increase  (e.g., standard RPA values may be poor indicators of
16      the economic benefits and costs produced by forest quality changes under,  say, alternative air
17      pollution regimes). The process of developing a tractable framework for ecosystem
18      management may require that valuation  studies also co-evolve to aid critical management
19      decisions.  For example, explicitly linking valuation techniques to physical resource functions
20      through bioeconomic models, remains an important research area (Adams et al., 1990a).
21      Linking valuation measures, from both market and nonmarket studies, to indices of biological
22      diversity is a fundamental challenge (e.g., Niese and Strong, 1992).
23           Ecologists have a  traditional  skepticism of attempts to assign monetary values to
24      ecosystem functioning,  due both to inherent limitations in BCA and the inadequacy of
25      quantitative information about ecological and social factors (Westman, 1977; Higgs, 1987).
26      Attempts to monetize environmental benefits are also seen as having an inherent "quantitative
27      bias"; poorly understood ecological functions are neglected, while traditional commodities
28      (outdoor recreation) are paid full attention (Foy, 1990).
29           A further question is whether TEV really  captures total value. Economists make no
30      claim that all values are being considered, only total economic  value.  But do traditional
31      measurement approaches really capture all economic value?  As Pearce (1993) states:

        December 1993                          5_269      DRAFT-DO NOT QUOTE OR CITE

-------
 1            There is in some sense a "glue" that holds everything together and that glue
 2            has economic value.  If this is true, and it is difficult to pinpoint what is at
 3            issue here, then there is a total value to an ecosystem or ecological process
 4            which exceeds the sum of the values of the individual functions.  Total
 5            economic value may not, after all, be total.
 6
 7          Can complex ecological functions be accurately expressed in monetary terms?  It is
 8     tempting to think that because of its inherent flexibility CVM may be up to the task (Russell
 9     1993).  The contingent valuation method has been applied to an impressive array of
10     nonmarket goods.  While the traditional focus has been on outdoor recreation, applications
11     include endangered species and unique  natural landscapes.  However, precise valuation of
12     ecosystem services with CVM will require a precisely defined commodity.  As researchers
13     move from valuing single environmental endpoints  or services to  addressing more complex
14     "bundles" of endpoints and services, it will become more difficult to define the commodity  in
15     a CVM survey.  This may prevent unambiguous estimation of such values.
16
17     Indirect Use Values
18          The common use/nonuse dichotomy may miss the fundamental interconnectedness and
19     transparency of complex ecological functions. The full range of ecosystem services is
20     comprised of multiple endpoints.  This vector of endpoints is supported by complex
21     interactions.  Uniqueness of the system lies in its functional structure, rather than discrete
22     environmental commodities—often the visual or spectacular—which satisfy human
23     preferences.  Within the TEV taxonomy,  indirect use values comes the closest to capturing
24     the system characteristics of complex ecological functions (Pearce, 1993).
25
26     Potential Misuse/Abuse of Economic Values
27          If understanding of functional structure of ecosystems is inadequate, then can any
28     attempt to express the valuation of ecosystem service flows be  satisfactory? While services
29     may indeed be important,  grossly imperfect attempts at monetary valuation may do more
30     harm than good (Norton, 1987; Rolston,  1988; Sagoff, 1988).
31           The first possibility is that precise quantification  may introduce  a degree of rigidity or
32     inflexibility that reduces the efficacy of future planning and management. There may be an
33     inherent need to  seize onto any monetary value, no matter how poorly measured. Once

       December 1993                          5-270      DRAFT-DO NOT QUOTE OR CITE

-------
 1      seized, the value can then take on a life of its own.  A second possibility is that focusing on
 2      satisfaction of preferences of the current generation and distributional status quo ignores
 3      other collective social priorities.  Examples include intergenerational equity and the notion of
 4      preserving critical natural capital (biogeochemical cycles, genetic information, etc.) embodied
 5      in the vast literature on sustainable development (Pezzey, 1992; Pearce,  1993).
 6           If attempts at assigning monetary  values are found to be unsatisfactory for the full
 7      complex of ecosystem service flows, then alternative decision rules must be given closer
 8      scrutiny.  One such decision rule is the often-discussed safe minimum standard.
 9
10      Safe Minimum Standard
11           The safe minimum standard (SMS) of conservation for ecosystem or other resources
12      which give rise to a steady stream of benefits or servcies ("flow resources") was originally
13      introduced by Ciriacy-Wantrup (1952).  The SMS is a decision rule to protect critical flow
14      resources unless the costs of doing so are intolerably large (Randall, 1989,  1991).  The SMS
15      rule is designed to provide flexibility and protect future options in the presence of true
16      uncertainty (where probability assessments cannot be meaningfully made), and the possibility
17      of irreversible ecological changes exist  (Westman, 1977).  Determination of "intolerable"  is a
18      social choice which  can be informed by both economists (by identifying  the costs associated
19      with alternative degrees of protection or preservation), and ecologists (by identifying
20      ecological indicators and threshold  effects which can be tied to preservation costs). The SMS
21      concept has received increasing attention (e.g., Bishop and Woodward, 1993; Randall, 1991)
22      and is closely linked to the notion of "critical natural capital" that occurs in some
23      formulations of sustainable development in agriculture and forestry.
24           Recent  discussions of the SMS to  threatened and endangered species applications
25      include Hyde (1989), Castle and Berrens (1993), and Stevens et al. (1991).
26
27      5.8.4.5  The Research Agenda
28           The previous sections highlight some deficiencies in the natural science and economics
29      literature which prevent valuation of ecosystem services.  This  section offers a  set of
30      opportunities for future research efforts to addresses these deficiencies.   No priority is
31      assigned and some opportunities are obviously overlapping.

        December 1993                           5-271      DRAFT-DO NOT  QUOTE OR CITE

-------
 1     (1985) suggests that the value of additional natural science information (in terms of reducing
 2     confidence materials around economic estimates) declines rapidly.  Thus, not all sources of
 3     uncertainty need be removed before economic analyses can proceed.
 4
 5     Explore Relationship of Ecosystem Functions and Service Flows to Economic Values
 6          An important research question is whether measures based on subjective preferences
 7     (e.g., stated WTP from a CVM study, or observed WTP from an HPM study) have any
 8     relationship to indices of ecosystem functions and service flows (Costanza et al., 1991).  For
 9     example, Hanley  and Ruffell (1993) find that "forest characteristics are in general poor
10     predictors" of recreational value in a CVM study.  However, they also conclude that the
11     chief problem lies in quantifying changes in natural science information.  Utilization of GIS-
12     based tools offer  new opportunities for connecting natural science information with a variety
13     of economic models.
14           A critical building block in identifying such connections is the development of a shared
15     language.  For example, the connections between the concept of "endpoints" for ecological
16     risk assessment and economic valuation are unclear.  The EPA (1992) framework for risk
17     assessment defines an assessment endpoint as:  "an explicit expression of the environmental
18     value that is to be protected."  However, as Suter (1990) makes clear, assessment endpoint,
19     "must be valued by society, but they are not ultimate values."  An important, but not the
20     sole, measure for expressing social value are economic values.
21          Future valuation studies may demonstrate that complex, and often transparent,
22     ecological functions do not map into individual preferences. This would appear to be useful
23     information worthy of documentation.  It would also not be a reason to discard experimental
24     techniques such as CVM.
25
26     Identify Limits to Application of Valuation Techniques
21          The measurement of nonuse values using the contingent valuation method remains
28     controversial. Given ethical limitations to markets in various social spheres (Anderson,
29      1990), there is a  limit to the things to which we can meaningfully assign values.  As one
30     example, the assignment of monetary values as  expressions of the worth of certain personal
31     or social relations may change the nature of  the relationship. As a second example,

       December 1993                          5-272      DRAFT-DO NOT QUOTE OR CITE

-------
 1      following Bishop and Woodward (1993), and Howarth and Norgaard (1992), we cannot
 2      expect nonmarket values to resolve large-scale sustainability and intergenerational equity
 3      issues.  Economic efficiency criteria provide no guarantee of the protection of any particular
 4      environmental assets (Foy,  1990) or ecological sustainability (Common and Perrings,  1992).
 5
 6      Identify the Degree of Substitutability Between Natural and Man-Made Capital
 1           Neoclassical economics has no traditional notion of sustainability other than
 8      intertemporal efficiency.  A critical issue in the  sustainability literature is the degree of
 9      substitutability between man-made and natural capital.  Substitutability can occur on several
10      levels.  The first question is whether man-made capital is an adequate substitute for the full
11      range of complex ecological functions.  The corollary question is the degree of
12      substitutability within the structure of human preferences. Valuation methods based on
13      willingness to pay and willingness to accept compensation assume an underlying
14      substitutability.  Economic values are exchange values based on the notion of indifference—
15      they express the terms of trade (money for environmental services) and money is the good
16      which accesses other exchange commodities. In short, assigning an economic value to
17      critical natural capital assumes an inherent substitutability for that asset in individual
18      preference functions.
19
20      5.8.4.6   Valuing Ecosystem Service Flows:  Summary
21           Economists have a variety of valuation techniques to help guide policy choices
22      concerning the effects of air pollution or other environmental change on environmental
23      assets.  Applying these techniques to ecosystem  management issues and valuing the full range
24      of ecosystem service flows is a new, and as yet, unresolved challenge. Current
25      state-of-the-art assessment methods are judged inadequate for environmental regulations.
26      Many scholars, in both ecology and economics,  are inherently skeptical of any economic
27      valuation of the full complex of ecosystem services, and turn towards other value indicators.
28      Costanza (1991) argues for methodological pluralism, where the imperfect information gained
29      from multiple approaches is combined in an integrated informational structure.  The
30      identified research agenda for valuing ecosystem service flows crosses traditional disciplinary
31      boundaries (Russell, 1993). Interdisciplinary dialogue, cooperation, and development of

        December  1993                            5_273       DRAFT-DO NOT QUOTE OR CITE

-------
 1     shared language are necessary for successfully designing future valuation experiments
 2     concerning ecosystem service flows, and determining the proper role for such valuation.
 3
 4     5.8.5   Summary
 5          The 1986 Criteria Document contained a review of assessments of the economic
 6     consequences of O3 on U.S. agriculture.  This section has evaluated selected post-1986
 7     literature on the same topic. In addition, the review has been expanded to include potential
 8     economic effects on forests and ecosystems.
 9          Based on economic assessments and scientific data available at the time, the previous
10     criteria document (U.S. Environmental Protection Agency, 1986) concluded that O3 at
11     ambient levels was imposing economic costs on  society. The review of more recent (post-
12     1986) literature on agriculture corroborates that  earlier conclusion.  Specifically, the recent
13     literature, using the full set of NCLAN data  and addressing some deficiencies in the pre-1986
14     assessments, confirms the finding of economic losses from ambient O3 concentrations.
15          The exact level of these economic effects is a function of cropping patterns,
16     O3 concentrations (both ambient and episodic), and the  spatial and temporal characteristics of
17     projected or observed O3 levels. The current economic assessments represent improvements
18     in the scientific understanding of O3 effects on agriculture.  However,  the assessments of
19     economic effects initially incident on the agricultural sector remains incomplete.
20          Only a few assessments consider the economic effects of O3 on forest trees as well as
21     urban trees, shrubs, and ornamentals.  These studies assess the economic effects of
22     hypothetical changes resulting from O3 or other stressors on forest productivity and aesthetics
23     and are best viewed as measures of the potential effect  of O3 on these  receptors.
24     Improvements linking O3 effects data to productivity and aesthetic effects will improve the
25     utility of such economic analyses.
26          The effects of O3 on ecosystems have not  been addressed in the published literature.
27     There is, however, an emerging interest in applying economic concepts and methods to  the
28     management of ecosystems.  Ecological research is also addressing the challenging
29     conceptual and practical issues in understanding and managing ecosystem functions.
30     Economic research continues to  develop, refine, and apply techniques  for valuing market and
31     nonmarket products and services that will be of help in estimating the  economic effects  of O3

       December 1993                           5-274     DRAFT-DO NOT QUOTE OR CITE

-------
  1      on ecosystems.  Increased dialogue between the disciplines is needed before empirical
  2      analyses of the economic consequences of ecosystem management are feasible.
  3           In summary, the state of science concerning O3 economic effects on agricultural crops
  4      is sufficient to conclude that O3 imposes costs on society.  Conclusions regarding effects on
  5      forests and ecosystems must await the acquisition of additional data and possible refinements
  6      in ecological and economic  methods.
  7
  8
  9      5.9   INTEGRATIVE  SUMMARY AND CONCLUSIONS FOR
 10            VEGETATION AND ECOSYSTEM EFFECTS
 11      5.9.1   Introduction
 12           Review of the post-1986 literature has not altered the conclusions of the earlier Criteria
 13      Document (U.S. Environmental Protection Agency, 1986)  or Supplement (U.S.
 14      Environmental Protection Agency, 1992).  In the 1986 criteria document,  several general
 15      conclusions were drawn from various experimental approaches:  (1) current ambient ozone
 16      concentrations in many areas of the country were sufficient to impair growth and yield of
 17      plants; (2) effects occur with only a few hourly occurrences above 0.08 ppm; (3) growth and
 18      yield data cited in the  1978  criteria document (U.S. Environmental Protection Agency, 1978)
 19      indicate several species exhibited growth and yield effects when the mean  ozone
 20      concentration exceeded 0.05 ppm for 4 to 6 h/day for at least 2 weeks; and (4) regression
 21      analyses of NCLAN data developing exposure-response functions for yield reductions
 22      indicated that at least 50% of the crops were estimated to exhibit a 10% yield reduction at
 23      7 h seasonal mean ozone concentrations of 0.05 ppm or less.  These conclusions remain valid
 24      today. The 1992 Supplement reviewed the literature concerning the appropriate exposure
 25      index for expressing O3 effects  on vegetation, including evaluation of the (1) role of
 26      exposure duration, (2)  the role of peak concentrations, (3) the 7- and 12 h mean
 27      concentrations, and (4) comparison of many possible exposure indices to summarize seasonal
 28      exposures and relate to yield loss.  It was concluded that the 7- and 12  h seasonal mean was
29      not appropriate because of its treatment of all concentrations equally, and the lack of
30      consideration  of exposure duration. Experimental studies had indicated the influential role of
31      episodic,  peak concentrations and the length of the exposure. A comparison of possible

       December 1993                         5.275      DRAFT-DO NOT QUOTE OR CITE

-------
 1     exposure indices concluded that the preferred indices cumulated all hourly concentrations
 2     during the growing season and preferentially weighted the higher concentrations.  These
 3     conclusions remain valid today.
 4           The review of the post-1986 literature has revealed additional analyses of the NCLAN
 5     database as well as several European crop yield loss studies, substantiating the effects
 6     observed in this country.  There has been only limited publication of experimental studies
 7     directly addressing the role of each of the exposure components to further our understanding
 8     of what should be appropriate exposure indices relating  ambient O3 concentration to effects.
 9     There have been, however, several retrospective analyses of NCLAN data that increase
10     confidence in the use of the peak-weighted, cumulative indices.  Studies of forest tree
11     seedlings have  substantiated pre-1986 studies indicating  the sensitivity of a number of
12     species, at least as  seedlings.  Data concerning the response of large mature trees as
13     individuals or in stands are limited.  Seedling growth response of some species is altered at
14     O3 concentrations observed in many areas of the United States.  Studies of the role various
15     biotic and abiotic environmental factors play in the response of plants to O3 indicate the
16     complexity of determining the response of plants in natural ecosystems wherein the
17     interaction of species, genotypes, and the multitude of environmental influences dictate the
18     eventual response of the species or community in question.
19
20     5.9.2   Species Response  and Ecosystem Response
21           Ozone injury was first observed on crop plants.  Therefore crop plants have been
22     studied more intensively than those plant species growing in natural habitats.  As a result,
23     most of the information concerning species response, to O3 comes from the studies of crop
24     plants.  The number of crop species/cultivars for which response data is available, however,
25     is a mere fraction of the total plants grown as crops.  This is especially true for native
26     herbaceous plants and trees where the studies are far fewer in number.  Because of the
27     known wide range of sensitivities to O3 among the species that have been studied and even
28     among cultivars of individual crops (see Section 5.4.2), it is not possible to estimate the
29     sensitivity of any given species and/or cultivar that has  not been investigated directly except
30     in very general terms.
        December 1993                           5-276      DRAFT-DO NOT QUOTE OR CITE

-------
 1          One attempt at using our fragmented knowledge to develop a general framework of
 2     response covering a range of species has been presented by Reich (1987).  He described a
 3     conceptual model for conifers, hardwoods and agricultural crops, based on considerations of
 4     the carbon balance and growth of individual plants in relation to O3 exposure or uptake
 5     (estimated from O3 concentration and stomatal conductance).  For equivalent exposures to
 6     O3 during a single growing season, he ranked these groups in order of decreasing sensitivity
 7     as: crops, deciduous hardwoods, evergreen conifers.  A similar ranking results when the
 8     published response data are reviewed.  The concentration of ozone causing yield  losses in
 9     crop species is slightly less than that observed to cause biomass reduction in deciduous
10     species.  A slightly greater concentration of ozone causes reductions in total biomass  in some
11     coniferous species.  However it  is important to note that the variation of this biomass
12     response within these large groupings by growth strategy is as great or greater than the
13     variation in response between the groups. Caution is also  needed with such generalizations
14     because these groupings compare annual versus perennial growth of long-lived species,  as
15     well as the influence on growth  response of a vast array of environmental factors at play on
16     these species in natural ecosystems.
17          The focus of research for developing quantitative relationships between O3 exposure
18     and biological effects has been on the response  of individual species for three reasons:
19     (1) Single species studies are achievable experimentally, including ease of developing
20     adequate experimental design and exposure technology.  (2) In many  instances  the plants are
21     grown in  monoculture (e.g., most crop plants, ornamentals, fruit and nut species, plantation
22     forests), and the inter-specific competition and diversity, which typifies natural communities
23     is not an issue.  The predicted response may also include the environmental influences of its
24     growing environment (e.g., drought) that modify the exposure-response relationship.
25     (3) In systems that are comprised of a multitude of species (e.g., mixed forest  stands,
26     pastures or grasslands) it is important to  understand the response of the individual
27     components so that behavior of the system might be analyzed in a systematic fashion.  The
28     underlying assumption is that understanding how a forest stand responds to O3  requires
29     knowledge of the response of each species within that stand as a starting point. The
30     interactions that typify the community are subject to O3 effects as well and may manifest
31     themselves as a measurable effect some time later as a  result of these interactions.  Up to this

       December 1993                          5-277       DRAFT-DO NOT QUOTE OR CITE

-------
 1     time, aside from the study of the San Bernardino forests, the holistic approach to
 2     understanding O3 effects has not been pursued.  Exposing large woody and herbaceous
 3     species growing in natural species assemblages and subjected to a large array of climatic and
 4     biotic environmental factors over decades has not been possible.
 5          It is important to note that there  may be a limited potential for using individual plant
 6     (species) responses to an environmental stress (such as O3 exposure) to predict population
 7     and community response (Woodward,  1992).  As one progresses from knowledge of a tissue
 8     or organ's stress-response to the whole plant, population, community and ecosystem levels,
 9     various feedback mechanisms may modify the propagation of the effect.  Important
10     components of such feedback are the mechanisms of homeostasis which involve  injury repair
11     (at the metabolic level) or various types of compensation (Tingey and Taylor, 1982).
12     Compensation, which may occur at all levels of organization, from the subcellular to  the
13     ecosystem,invokes processes that counteract the detrimental effects  of the stress. At the
14     ecosystem level, an effect on the growth rate of a particular species may not be  translated
15     into a comparable effect on the growth rate of a population  of the species,  because of
16     changes in the intensity of competition (Woodward, 1992).
17          At the present time, most of our knowledge of O3 exposure concerns the effects on
18     individual plants or their parts. Although we have  some information about effects at the
19     population level with some agricultural crops and some forest tree populations, the
20     information regarding the propagation of effects upward through the different hierarchical
21     levels within natural and forest ecosystems is limited.
22
23     5.9.3   How Does Ozone Affect Plants?
24          Plant growth and yield are the product of a series of biochemical and physiological
25     processes related to uptake, assimilation and translocation of ozone in the individual plant.
26     Ozone exerts a phytotoxic effect only  if a sufficient amount reaches the sensitive cellular sites
27     within the leaf.  To do this, it must diffuse from the ambient air into the leaf through the
28     stomata, which exert control  on O3  uptake.  Ozone effects will not occur if (1) the rate of
29     ozone uptake is low enough that the plant can detoxify or metabolize O3 or its metabolites;
30     or (2) the plant is able to repair or compensate for the effects.  Cellular disturbances  that are
31     not repaired or compensated are ultimately expressed as visible injury to the leaf and/or

       December 1993                          5-278      DRAFT-DO NOT QUOTE OR CITE

-------
  1      effects on growth, yield, or both (Tingey and Taylor, 1982; U.S. Environmental Protection
  2      Agency,  1986).  Ozone effect is cumulative, resulting in net reductions in photosynthesis,
  3      changes in allocation of carbohydrate, and early senescence, which leads to reductions in
  4      biomass and productivity, and alterations in susceptibility to abiotic and biotic stresses and/or
  5      decreased reproduction.
  6           Ozone is expected to reduce growth or yield only if (1) it directly impacts the plant
  7      process that is limiting to plant growth (e.g. carbon fixed); or  (2) it impacts another step
  8      sufficiently so that it becomes the step limiting plant growth (e.g., allocation of
  9      carbohydrates to roots and nutrient uptake becomes limiting to plant growth) (Tingey, 1977).
10      Conversely, O3 will not limit plant growth if the process impacted by O3 is not growth-
11      limiting.  This implies that not all effects of O3 on plants are reflected in growth or yield
12      reductions.  These conditions also suggest that there are combinations of O3 concentration
13      and exposure duration that the plant can experience that may not result in visible injury  or
14      reduced plant growth and yield (U.S. Environmental Protection Agency,  1986).  However,
15      subtle physiological effects which may not result in immediate growth reductions may result
16      in increased plant susceptibility to other environmental factors  and competition.
17           The mode of action of O3 on plant species described in the 1986 criteria document
18      (U.S. Environmental Protection Agency, 1986) still holds true. The plant leaf is the site
19      O3 action and the critical effect is on the plant's carbon  budget (the amount of carbohydrate
20      produced). Inhibition of photosynthesis limits  carbohydrate production and allocation
21      resulting  in reduced biomass, growth and yield.  Studies since  1986 corroborate this
22      understanding, adding information on the effect of O3 on photosynthetic capacity, respiration,
23      leaf dynamics, and on the detoxification and compensatory  processes.  In particular, exposure
24      to O3 concentrations at or near current ambient levels (see Table 5-17 Section 5.6) has an
25      effect on  photosynthesis, but a longer exposure duration is necessary to produce a growth
26      response, taking days to weeks rather than hours as in earlier studies with higher
27      concentrations (0.25 ppm  or greater).  The loss of leaves prematurely as a result of
28      O3 exposure  has been observed in several species  and is particularly important in coniferous
29      tree species.  This O3-induced loss in leaf area can be a  significant factor in the reducing the
30      amount of carbohydrate produced by the plant.  Both a reduced photosynthetic capacity and a
31      reduced leaf area contribute to the reduction in carbohydrate production by plants.  However,

        December 1993                           5.279      DRAFT-DO NOT QUOTE OR  CITE

-------
 1     the mechanism of premature senescence is not understood.  In addition to leaf loss, reports of
 2     stimulation of production of new leaves and higher photosynthetic capacity of new leaves
 3     represent compensation processes that operate in some species of trees. These mechanisms
 4     may counteract the reduction in canopy carbohydrate production resulting from O3.  Some
 5     quantitative understanding of these processes is needed to be able to predict long-term effects
 6     of O3 on tree  species.  More information is needed as well in understanding O3 uptake at the
 7     canopy level and how the plant integrates the effects of 63 to enable prediction of long-term
 8     effects of O3 exposure in ecosystems, i.e., species response as a function of interactions with
 9     other species,  abiotic and biotic environmental factors.  Unfortunately, there is little
10     experimental evidence to date regarding effects of long-term O3 exposure on perennial plants.
11     Few experimental  studies have extended exposures beyond one season and only in a limited
12     number of studies  have observations of growth been extended into the following year, thus
13     observing "carry-over" effects in several tree species. These carry-over effects are
14     significant to long-lived species such as trees since they affect the elongation of new spring
15     shoots or root growth in the year following exposure to O3.  In at least one instance this has
16     been correlated with reduced storage carbohydrate in roots.  The implication of these effects
17     on long-lived  species is significant.  Reduction in growth and productivity, a result of altered
18     carbohydrate produced and allocated, may appear only after a number of years or when
19     carbohydrate reserves in the tree are depleted below  some threshold concentration.
20
21     5.9.4   Factors That Modify Plant Response to Ozone
22           Plant response to O3 exposure is modified by factors within and external to the plant
23     species; cultivars and individuals within populations display variable response to O3.  The
24     plant's response and the variation of that response is dictated by genetics and the plant's
25     present and past environmental milieu.  The environment includes biotic and abiotic factors
26     of the species' growing environment, the temporal pattern of exposure concentrations, and
27     the plant's phenotypic stage during exposure.
28
29      5.9.4.1   Genetics
30           An important component of this variation is genetically controlled.  The specific genes
31      controlling O3 response and  involved in mechanisms of O3 tolerance are as yet largely

        December 1993                           5-280      DRAFT-DO NOT QUOTE OR CITE

-------
  1      unknown. However, control of stomatal conductance and internal biochemical defense
  2      systems are among the most commonly described tolerance mechanisms.  Ozone tolerance is
  3      generally thought to be controlled by multiple genes.  The implications of genetic variation
  4      for managed and natural ecosystems are several-fold: (1) The potential for natural selection
  5      for O3 tolerance and associated loss of sensitive genotypes is regional in nature, unlike well
  6      known point-source pollution impacts which occur on local plant populations.  However, the
  7      intensity of O3 selection is generally thought to be quite low, 0.3 or less (Taylor and Pitelka,
  8      1992) across most U.S. areas.  (2) While it is known that individual plants within a species
  9      vary in their O3 tolerance, the physiological costs to tolerant plants are not known in terms
 10      of carbohydrate assimilation (energy production) and allocation. Tolerance mechanisms
 11      based on reduced stomatal conductivity in the presence of O3 would likely reduce the growth
 12      of tolerant plants.  Similarly, tolerance mechanisms based on the productivity of antioxidant
 13      compounds will likely shunt plant resources away from growth to the production of the
 14      defense compounds.  (3) Exposure-response equations and yield-loss equations developed for
 15      a single or small number of cultivars, genotypes, families or populations may not adequately
 16      represent the response of the species as a whole.  As a corollary to this, the sensitivity of
 17      responder genotypes can not be determined  by measuring effects just in relation to mean
 18      O3 concentrations.
 19
 20      5.9.4.2  Environmental Factors
 21           Since the previous criteria document (U.S. Environmental Protection Agency, 1986),
 22      additional studies have been published on a  wide range of biological, physical, and chemical
 23      factors in the environment that interact with plant response to O3. While understanding the
 24      plant's response to O3 requires an understanding of the role of environmental factors that
 25      modify that response (primarily to reduce uncertainty in the estimation of species' exposure-
 26      response), the corollary is also important to understand, and in fact has not received as much
 27      attention, i.e., the exposure to  O3 can modify the plant's ability to integrate its environment.
28      For example, exposure to O3 reduces the tree's ability to withstand winter injury caused by
29      exposure to freezing temperatures and influences the success of pest infestations.
30           Biological components of the environment of individual plants include pests, pathogens
 31      and plants of the same or other species in competition.  With regard to insect pests, although

        December 1993                           5_281      DRAFT-DO NOT QUOTE OR CITE

-------
 1     only a very limited number of plant-insect systems have been studied, there is a general trend
 2     in the observations which suggests that some pests have a preference for and grow better
 3     when feeding on plants that have been impacted by O3, but there is no evidence to suggest
 4     that O3 may trigger pest outbreaks. Unfortunately, because we have no knowledge of how
 5     the vast majority of plant-insect systems will be affected by O3, it is not possible to offer any
 6     quantitative overall assessment of the  consequences of such interactions on the growth of
 7     crops and natural vegetation.  At best, we may conclude that there is a reasonable likelihood
 8     that some insect pest problems will increase as a result of increased ambient O3 levels.
 9     Indeed, this was seen in  the San Bernardino Mountains where ponderosa pine experienced
10     bark beetle infestations with higher O3 exposures (U.S. Environmental Protection Agency,
11     1986).
12           Plant-pathogen interactions also  appear to be affected  by O3.  The suggestion that
13     diseases caused by obligate pathogens tend to be diminished by O3 while those caused by
14     facultative pathogens tend to be favored (Dowding, 1988), is generally supported  by the
15     limited evidence available. In terms of its broader implications, this suggests that continued
16     exposure to O3 may lead to a change  in the overall pattern  of the incidence and severity of
17     specific plant diseases affecting crops and forest trees.
18           With regard  to the physical environment, the combination of light, temperature and
19     water availability largely determines the success of plant growth because of the influence of
20     these factors on the processes  of photosynthesis, respiration and transpiration. For
21     agricultural crops,  perhaps the most important of these potential interactions with
22     O3 concerns water availability and use.  There is consistent evidence that severe drought
23     conditions tend to reduce the direct adverse effects of O3 on  growth and yield.  Conversely,
24     the ready availability of soil water tends to increase the susceptibility of plants to O3 injury.
25     However,  a lack of water should not  be viewed as a potentially protective condition, because
26     of the adverse effects  of drought per  se.  With perennial trees, there is some evidence that
27     prolonged exposures to O3 may lead  to greater water use efficiency  which may enable such
28     trees to be better able to survive drought conditions.
29           The plant's environment also contains numerous chemical components,  ranging from
30      soil nutrients and  other air pollutants to agricultural chemicals used for pest,  disease and
31      weed control.

        December 1993                          5-282     DRAFT-DO NOT QUOTE OR CITE

-------
 1           A large number of studies have been conducted on the effects of O3 in conjunction
 2      with other gaseous air pollutants such as SO2 and NO2, although the information obtained in
 3      several of the studies is of no more than academic interest because of the unrealistic exposure
 4      conditions used.  Preliminary evidence suggests that nitrate deposition in the soil could
 5      influence plant response to O3.
 6           Since increased tropospheric O3 is a component of global climate change, results from
 7      studies on the interactions of O3 with increased levels of CO2 and UV-B radiation are
 8      beginning to appear.  Initial work with CO2 suggests that increased CO2 levels may
 9      ameliorate the effects of O3.   However, it is too soon to be able to  generalize on the outcome
10      of this interaction.  At the present time, no investigations of the compound interactions
11      involving O3, CO2, UV-B, increased temperature and changed soil  moisture status have been
12      reported.
13           In conclusion, in spite of the amount of work carried out to date on the interactions of
14      O3 with environmental factors, there is not a strong quantitative database to generalize and
15      extend the effects of O3  on species across environments. Uncertainty about the extent of
16      modification of the exposure-response relationship as a result of different growing
17      environments remains, as well as the uncertainty associated with understanding O3's role in
18      altering a species' ability to integrate its environment.
19
20      5.9.5   Exposure Dynamics
21            The effects of O3 on individual plants  is not only a function of inter-  and intra-
22      specific differences in tolerance (genetics), and growing environment affecting the uptake of
23      O3 (e.g., soil water, nutrient), but also the characteristics of the exposure itself which affect
24      the uptake of O3  from ambient air, and thus the ultimate growth response. From the studies
25      prior to 1986 and after 1986, evidence indicates that the components of exposure, i.e. peak
26      concentration, frequency of occurrence and duration, play various roles in the plant response.
27      The temporal pattern of hourly concentrations in the exposure influence the response.  There
28      is a reported greater influence on growth in annual and perennial crop species (bush beans
29      and alfalfa),  and  in tree seedlings  (ponderosa pine  and aspen) of episodic peak exposures
30      compared to either daily peak occurrences in the case of crops or non-diurnal, continuously
31      elevated exposures typical of remote regions in the case of tree seedlings. The results

        December 1993                          5_283       DRAFT-DO NOT QUOTE OR CITE

-------
 1     suggest a variation in the growth response of species as a function of the dynamics of the
 2     exposure.  In addition to the temporal distribution of concentration during a day and during a
 3     season, there is also the distribution of the exposure during the growing season and the
 4     phenology  of the plant.  Some phenotypic stages of growth are more sensitive to O3 than
 5     others.  In  most instances of crop exposure studies, in particular the NCLAN database, the
 6     exposure treatments used in developing response functions have used ambient concentrations
 7     as a base.  Thus, the variation in the response as the result of a variation in regime type is
 8     not known. The same reservation is applicable to the growth response reported for tree
 9     seedlings.  It is not possible at this time to quantify the alterations in the growth or yield
10     response as a result of different exposure patterns.  However, it is possible to suggest which
11     components of an exposure play a relatively greater influence in growth alterations than do
12     other components of the exposure.  For example, peak concentrations are more effective than
13     lower concentrations in altering growth; and the episodic occurrence of peak  events seems to
14     be more damaging than the daily occurrence of the same peak value or a continually elevated
15     concentration over a growing season.  The variation in species' response as a function of
16     exposure concentration and duration suggests the importance of a measure of the ambient air
17     exposure to relate to the biological effects.
18
19     5.9.6   What Measure of Exposure Characterizes Species Effects?
20           A measure is needed to relate ambient exposure to the observed biological effect(s).
21     The amount of O3 taken up from the atmosphere by the plant (either rate of uptake or
22     cumulative seasonal uptake) is the ultimate measurement of O3 exposure, but this is not a
23     practical measure to make directly.  The uptake rate and total cumulative uptake can be
24     calculated  from ambient concentrations and species' gas exchange characteristics.   A measure
25     of uptake integrates all those environmental  influences on stomatal conductance controlling
26     the effect,  e.g., temperature, humidity, soil  water status, etc., but it is not practical for most
27     experimental approaches used in determining what ambient concentrations of O3 can be
28     tolerated by vegetation.   Thus an  index of ambient exposure is required as a  surrogate of
29     uptake.  Any  index that relates well to plant response  should incorporate these environmental
30     and exposure  dynamic factors, directly or indirectly, in weighting the hourly
31     O3 concentrations differentially.

       December 1993                           5-284       DRAFT-DO NOT QUOTE OR CITE

-------
  1           Given the evidence suggesting a relatively greater contribution to effects of higher
  2      concentrations, episodic occurrence of peak concentrations, and the duration of the exposure,
  3      an index that cumulates hourly concentrations during the season and gives greater weight to
  4      the higher concentrations appears to be an appropriate index for relating ambient exposure to
  5      growth or yield effects.  A number of different forms of a peak-weighted, cumulative index
  6      have been examined, e.g., SUM06, SIGMOID, W126, for their ability to properly order
  7      yield response in the large number of crop yield studies of NCLAN.  All perform equally
  8      well and it is not possible to distinguish between them on the basis of statistical fits of the
  9      data.  In retrospective analyses when O3 is the primary source of variation in response, year
10      to year variations in plant response are minimized by the peak-weighted,  cumulative exposure
11      indices.  No experimental studies, however, have been designed specifically to evaluate the
12      adequacy of the various peak-weighted indices.
13           This document's conclusions are  no different than those of the 1986 criteria document
14      or the 1992 Supplement (U.S. Environmental Protection Agency, 1986, 1992):  (1) mean
15      indices are not among the best exposure indices; and (2)  the preferred indices are those
16      cumulating hourly values over the growing season and preferentially weighting the peak or
17      higher concentrations.
18           The 7- and 12-h seasonal means were earlier indices used to describe plant response.
19      The mean indices have been  shown to  be inadequate in ordering growth response in
20      experimental studies as well as retrospective analysis of NCLAN data (U.S.  Environmental
21      Protection Agency, 1986). This is not surprising since a mean index implies that all
22      concentrations are equal in their effect on plants,  and does not consider duration of exposure.
23      Exposure duration is influential in the response,  as well  as the timing of exposure during a
24      growing season coinciding with sensitive plant growth stages.  Phenology is one factor, other
25      than peak events and duration, that is influential in response.  Others such as respite time,
26      canopy structure, environmental conditions, e.g.,  soil and nutrient conditions, are considered
27      important but not well understood.  All these factors interact with concentration and duration
28      in different fashions depending on species.  The peak-weighted cumulative indices do a better
29      job of considering at least a part of this information on environment, phenology, etc., than
30      the mean  or  single-event peak indices,  because of their inclusion of concentration weighting
31      and duration. Recently, the mean O3 flux was used as an index and it minimized the year  to

        December 1993                          5_2g5      DRAFT-DO NOT QUOTE OR CITE

-------
 1     year variation in response when combining replicate studies, indicating the importance of
 2     environmental conditions in quantifying the relationship between O3 exposure and plant
 3     response.
 4     5.9.7   What Is the Estimated Crop Yield or Biomass Change with Ozone
 5              Exposure?
 6           In the 1986 criteria document (U.S. Environmental Protection Agency, 1986) and its
 7     supplement (1992) a distinction was made between foliar injury and damage. Yield loss was
 8     defined as an impairment in the intended use of the plant.  This concept included reductions
 9     in aesthetic values, foliar injury (changes in plant appearance), and losses in terms of weight,
10     number, or size of the harvested plant part.  Yield loss may also  include crop quality.
11     Losses in aesthetic values are difficult to  quantify. Foliar injury  symptoms can substantially
12     reduce the marketability of ornamental plants or crops where foliage is the plant part (e.g.,
13     spinach, lettuce, cabbage), and they constitute yield loss with or without concomitant growth
14     reductions.  It should also be recognized  that foliar injury to vegetation in national parks
15     constitutes reduction in aesthetic  value.  At that time  (1986), most studies of the relationship
16     between yield loss and O3 concentration focused on yields as measured by weight of the
17     marketable organ of the plant. From this perspective, damage can be segregated into several
18     categories:  (1) economic; (2) ecological  value of structure and function; (3) genetic
19     resources; and (4) cultural values (Tingey et al., 1990).  In the instance of crop species, the
20     effect of interest was yield, at least in the NCLAN research program.  In the instance of tree
21     species, much of the research has sought to measure  changes in biomass or productivity,
22     which could relate to all four of the above effect categories.
23           Diverse experimental procedures, ranging from field exposures without chambers to
24     open-top chambers and to exposures conducted in chambers under highly controlled climates,
25     have been used to study effects on crops  and tree seedlings. In general,  the more controlled
26     conditions are most appropriate for investigating specific responses and for providing the
27     scientific basis for interpreting and extrapolating results. These systems  are powerful tools
28     for adding to an understanding of the biological effect of air pollutants.  However, to assess
29     the economic  impact of O3 on crop yield or biomass  partitioning  in tree species, exposures
30     should have minimum deviations from the typical field environment in which the plant is
31     grown.  Much of the data reviewed in this document and in the 1986 ozone criteria document

       December 1993                           5-286     DRAFT-DO NOT QUOTE OR CITE

-------
 1     (U.S. Environmental Protection Agency, 1986) utilized the open-top chamber methodology.
 2     This approach has been the primary methodology for developing the empirical database of
 3     O3 effects on crop yield during the last 15 years. These are used because of the control they
 4     offer over exposures and still offer some semblance of relevance to field condition, and the
 5     ability to replicate studies from year to year. The NCLAN studies used sufficient treatments
 6     to allow development of exposure-response functions and became the largest database
 7     available for establishing a quantitative relationship between exposure and biological effect in
 8     crop and tree species  (as  seedlings). The response functions allow estimations and
 9     generalizations of biological response to O3 unlike information from multiple comparisons.
10          Two different approaches to re-analysis of NCLAN data have occurred.  The National
11     Crop Loss Assessment Network studied the major agronomic crop species,including corn,
12     soybean, wheat,  cotton, bean,  and alfalfa,  as well as several other regionally important
13     species accounting for 70% of all crop land in the United States and 73% of the agricultural
14     receipts. One approach estimated yield reduction of up  to 20% at 12 h seasonal mean of
15     0.06 ppm and a  10%  reduction at 0.045 ppm.  In another approach, they compared estimated
16     yield reduction in 54 studies and 12 crop species with 3 measures of exposure.  The average
17     duration of the studies was 74 days. It was concluded that 50% of the crops would
18     experience  10%  yield reduction at a 3  mo  Sum06 concentration of 26.4 ppm-h,  7 h seasonal
19     mean of 0.049 ppm, or a 2HDM of 0.094 ppm.  These  are averaged yield losses for all
20     species; more sensitive species would experience greater yield  losses at these concentrations.
21     The SUM06 has been examined in many papers; therefore, it has been used as an example in
22     the discussions of O3  effects that follow.
23          Similar results have been reported from European crop studies. Wheat yields were
24     reduced up to 29% depending  on the exposure and cultivars, but in no instance  were
25     O3 concentrations greater than a 0.062 ppm 7 h seasonal mean.  Spring rape yields were
26     reduced 9 to 26% at 8 h seasonal means of 0.03 to 0.06 ppm.   Seasonal 7 h means of
27     0.045 ppm  reduced bean yields 17%.

28     5.9.8    Ozone Concentration Across the United States
29          The O3 concentrations causing 10% or greater yield reductions in crop species are
30     concentrations that are not atypical of  O3 air quality during the past  10 years across the U.S.
31
       December 1993                          5_287      DRAFT-DO NOT QUOTE OR CITE

-------
                    1 - Eastern Seaboard
                    2 - Appalachian Highlands
                    3 - Greatiakes and Ohio Valley
                    4 - Interior Plains
                    5 - South
                    6 - Intermountain
                    7 • Southern California
                    8-North Pacific Coast
       Figure 5-27.  Regions of the United States for analysis of trends of ozone concentration.
                              1.E«m«nS««bo
-------
                                                        3.QM LAM M OHf V«ly
                         r:
                            J.i
i:
i •
i •
i:
                                                      i:
                          i:
                                1
                         i"
                         2 -jo
            i:
            i.
            i
            r:
               i:

                         i:
-V*
               i
      Figure 5-29. Ten-year trends in 5-mo 24-h SUM06 values by region at rural monitoring


                  sites.
                                                        i QTNI LAM and Ohio Vall^
                      i  0,

                      1^

                      2 -«.«
          •f -0.« J ttttMMMI/MWnm


          *       VMT
                           4.lnt»rtor PWrw
                       0.02




                       0.0) .
                           JL_
                                      I"

                                      J~


                                      j««
                                          « Nodh Pwnc oow
                                                      T«vYiv2nd Hlgtmt Mly Muc Aw*p
                                                                 ll
      Figure 5-30. Ten-year trends in second highest daily maximum values by region at


                  rural monitoring sites.






1     values estimated to cause 10% or greater yield losses in at least 50% of the crops are



2     exceeded in every year regardless  of exposure index.  The average among years for the 3 mo
      December 1993
                5-289
               DRAFT-DO NOT QUOTE OR CITE

-------
 1     using SUM06 is 29.5 ppm-h, 0.054 ppm 7 h seasonal mean, and 0.113 2HDM (Table 5-17;
 2     Section 5.6).  Both the seasonal mean and peak index (2HDM) were shown to be inadequate
 3     indices of exposure to relate to biological effects, but the values are given here for
 4     comparison since these are frequently used to express air quality or relate plant exposure
 5     effects.
 6          Trends and year-to-year variation in regional exposures are expressed as peak-weighted,
 7     cumulative indices (SUM06) for 3 or 5 mo (Figure 5-28 and Figure 5-29) and the event-
 8     based second highest daily maximum (Figure 5-30). The O3 concentration is variable from
 9     year to year during the 10 year period; and depending on the region of the country, each
10     year exhibits variation to a more or less greater extent from the 10 year average.  In the
11     Eastern Seaboard (Region 1) 1983 was well above the 10 year average.  Several  regions
12     show 1988 as the highest O3 year.  In the west, variation between years, and deviation from
13     the 10 year average is not as great  as in the east and the south. The 10 year averages for
14     only rural sites are generally higher that those using all O3  monitoring sites (includes urban,
15     as well as near-urban designations). All but 3 regions, the Interior Plains, Intermountain,
16     and Pacific Northwest, have average exposures greater than estimated to cause crop yield
17     losses  greater than 10% for 50% of the crop species, i.e.,  >  29 ppm h 3-mo SUM06
18     (Figure 5-28).  There does not appear an obvious trend in direction of O3 concentration by
19     either of the exposure indices, but the year-to-year  variation is great in several of the regions
20     and for most regions of the country 1983 and 1988 were noteworthy 'high O3' years.  This
21     variation in exposure would effect plant growth and is "coupled" to climatic conditions of
22     that year, all of which are important growth factors in plants.
23
24     5.9.9   What Are the Exposure Effects on Other Species—Trees and
25              Ornamentals?
26          Quantifying exposure-response in perennial plants (e.g., pasture grasses, shrubs, trees)
27     is complicated by the fact that they can receive multi-year exposures and because the results
28     of exposures in a previous year or  over a number of years  may be cumulative. Yield of
29     multiple year forage  crops (e.g., alfalfa and forage  mixtures), as with single season crops,
30     are reduced at concentration at or near ambient (0.04 to 0.06 ppm  12-h mean) in many parts
31     of the growing areas for these crops.  The question of cumulative effects from year to year

       December 1993                         5-290     DRAFT-DO NOT QUOTE OR CITE

-------
 1     has been addressed in only one instance (a two year alfalfa study in southern California) and
 2     there was no indication of such carryover effects (Temple et al., 1988a).
 3           As in the case of perennial crops, there is very little experimental evidence of the long-
 4     term effects of O3 on trees and shrubs. There  are studies reported in the earlier criteria
 5     document (U.S. Environmental Protection Agency, 1986) documenting sensitivity of
 6     seedlings in chambered exposure studies, but little information can be garnered from these
 7     studies regarding  biomass or productivity.  Recent exposure studies of black cherry and
 8     aspen suggest these are sensitive species and may have annual biomass changes  with current
 9     ambient concentrations of O3  in the regions where they are indigenous.  In an interesting
10     observation, 30-year-old red oak was reported to have 41 % reductions in canopy weight after
11     177 days exposure to a 7 h mean of 0.069 ppm, but  seedlings were not affected by this
12     exposure (Samuelson and Edwards, 1993).  A number of species, as seedlings, may be
13     experiencing biomass loss as indicated by a compilation of results of a number of deciduous
14     seedling studies (Figure 5-21; Section 5.5 and Table  5-26; Section 5.6) that indicate 10%
15     biomass  loss in 50%  of the seedling studies at concentrations of 31.5 ppm h (SUM06 in
16     92 days) or 0.055 ppm (7 h mean).
17           Exposure-response functions for 11 species of trees as seedlings indicate total biomass
18     losses in some species at  concentrations of O3 currently experienced in many regions  of the
19     United States. At concentrations of 33.3 ppm h for 92 days total biomass losses of 10%
20     would be predicted to occur for 50% of these seedlings.  When considered by growth
21     strategies, deciduous species appear to be more sensitive  that evergreen species and less
22     sensitive than most crops species on the basis of estimated annual biomass or yield loss.
23     A 10% annual biomass loss in deciduous species is estimated for 7 h mean of 0.055 or a
24     SUM06 of 31.5 ppm h compared to 0.049 7 h  mean and 26.4 ppm h causing 10% reduction
25     in yield of 50% of the crops.
26            Changes in biomass of evergreen forest  species, such as ponderosa pine,  loblolly and
27     slash pine are evident from the limited exposure studies of 03 at or near concentrations
28     typical of ambient (Table 5-17; Section 5.6) during a growing season (0.04 to 0.05 ppm 7 h
29     seasonal  means and 20 to 30 ppm  h SUM06 for 92 days). Estimated biomass loss of 10% in
30     50%  of the conifer seedlings examined occurs at a SUM06 92 day exposure of 42.6 ppm h.
       December 1993                          5-291      DRAFT-DO NOT QUOTE OR CITE

-------
 1          The effects of O3 exposure on fruit and nut tree species have received limited study.
 2     There are reported growth reductions in almond, pear, plum and apricot at 12 h means of
 3     0.051 ppm.
 4          Like crop species, tree species exhibit a wide range of response, depending on species,
 5     and genotypes within species.  Alterations in gas exchange, needle retention, carbohydrate
 6     reserves, root growth and total biomass and  productivity are reported.  Like other perennial
 7     species, the alteration by O3 of processes that alter total carbohydrate produced by the the
 8     canopy (i.e., photosynthetic capacity, needle retention), results in shifts in carbon allocation
 9     priorities and changes in growth.  In particular, root growth is often observed to be reduced
10     while shoot growth is maintained.  This reduction in root growth can result in reduced water
11     and nutrient uptake by  seedlings thus reducing seedling establishment.  Overall changes in
12     carbon budgets as a result of O3 exposures can hypothetically result in long-term changes in
13     growth.  However, most of the experiments  are conducted on seedlings and during 1 to
14     3 seasons, only 2% or less of the life span of the tree.  Whether or not these exposure-
15     response functions for  seedlings are representative of the larger, mature tree is unknown at
16     present.  Thus, the long-term effects are unknown and will undoubtedly require model
17     simulations.
18          Furthermore, because of the long life span of trees, there is ample opportunity for a
19     long-term cumulative effects on growth.  Small changes (even less than 1 to 2%  biomass loss
20     per year) which may not be detectable  statistically, might be translated into large changes
21     during the life span of the tree, and may result in changes in stand dynamics, with
22     concomitant effects on the structure and function of the ecosystem. The implication of these
23     effects on long-lived species is significant.  Reduction in growth and  productivity, a result of
24     altered carbon fixed and carbon allocated, may appear only after a number of years or when
25     carbohydrate reserves are depleted. Consideration must also be given to the fact that most of
26     these trees grow as part of mixed forests, in competition with many other species.
27
28     5.9.10   Spatial Characterization of Ozone  Effects
29           As reported for reductions in crop yield, tree species biomass reductions, based on
30     seedling growth response, have also been reported at concentrations of O3 currently
31     occurring in regions of the United States. The decade average 3  mo SUM06 is 29.5

       December 1993                           5-292       DRAFT-DO NOT QUOTE OR CITE

-------
  1      (Table 5-17; Section 5.6), only slightly below the 31.5 ppm h value estimated as capable of
  2      causing a 10% annual biomass loss in 50% of the deciduous species examined in seedling
  3      studies.  Individual species, such as black cherry or aspen,  would be estimated to experience
  4      10%  biomass loss at much lower concentrations, 16 to 20 ppm-h 3 mo SUM06 (Table 5-25;
  5      Section 5.6).  These concentrations are exceeded in those regions of the U.S. where these
  6      species occur (Figure 5-28).  Although the 10% annual biomass loss in conifers was
  7      estimated to occur at a 3 mo SUM06 of 42.6 pm h, this O3 exposure is higher than the
  8      decade average O3 in the U.S., but this concentration has been experienced in at least one
  9      region of the U.S. and in certain years, e.g., 1988, in several regions (Figure 5-28).
10           The spatial variation of ambient O3  exposure across the U.S. and the distribution of
11      crop  or tree species can be depicted visually in maps using the Geographical Information
12      System (GIS), and the effects of O3 characterized in a geographical  context by providing
13      some estimate of the spatial extent of current ambient O3 exposures  to vegetation (and the
14      variation about that estimate). Such approaches have been used for  the crop species studied
15      in NCLAN (Tingey et al.,  1991, 1993) and a number of forest tree  species as seedlings
16      (Hogsett et al., 1993). These spatial characterizations have combined estimates of
17      O3 exposure from the AIRS monitoring network, geographical distributions of individual
18      crop  and tree species' growing regions, and the exposure-response functions developed for
19      each  species.  The crop maps of Tingey et al. (1993) were revised using estimates of
20      O3 exposure developed by Herstrom et al. (1993) which estimate O3 concentration across
21      non-monitored areas.  To illustrate year-to-year variation in exposure, 1988 and 1989
22      monitored O3 concentrations reported as maximum 3 mo SUM06 are shown in Figure 5-31.
23      The maps of the estimated O3 exposure from these two years is shown in Figure 5-32.  The
24      peak  index, 2HDM,  is illustrated for the years 1988 and 1989 in Figure 5-33.
25           Exposure-response functions combined with the O3 exposure result in a spatially-
26      distributed yield loss. The year-to year variation in the estimated  yield reduction for all
27      crops is shown in Figure 5-34. Individual crop species soybean and wheat estimate with
28      yield  losses from 1988 are shown in Figure 5-35.  Tree species distribution and variation in
29      estimated total biomass reduction due to spatial variation in  O3 exposure are mapped in
30      Figures 5-36 to 5-38. As with crop species, these maps show possible exposures for each
31      species based on its distribution.  An example of year-to-year variation in exposure-response

        December  1993                          5.293      DRAFT-DO NOT QUOTE OR CITE

-------
        A. Monitored 3 Month SUM06 Exposures (1988)
                                                    ppm-hrs
                                                       <20
                                                       20-40
                                                       40-60
                                                       >60
         B. Monitored 3 Month SUM06 Exposures (1989)
Figure 5-31.  A) 1988 ozone monitoring site locations and calculated 3-mo SUM06 at
           each site.  B) 1989 ozone monitoring site locations and 3 mo SUM06 at
           each site.  AH sites regardless of landscape designation included.
December 1993
5-294
DRAFT-DO NOT QUOTE OR CITE

-------
            A. Estimated 3 Month SUM06 Exposures (1988)
                                                        pj>m-hrs
                                                          <20
                                                          20-40
                                                          40-60
                                                          >60
             B. Estimated 3 Month SUM06 Exposures (1989)
Figure 5-32.  Estimated ozone exposure across the eastern half of the United States for
            1988 (A) and 1989 (B). SUM06 exposure values based on actual
            monitoring regions based on the regression relationship with the exposure
            potential surface.

Source: Herstrom et al. (1993).
December 1993
                                   5-295
DRAFT-DO NOT QUOTE OR CITE

-------
              A. (1989)
                                                           2HDM
                                                                0.09
                                                               L10-0.11
                                                              0.12-0.13
                                                              >0.13
             B. (1988)
                                                          2HDM
                                                          d 0-0.09
                                                          [^ 0.10-0.11
                                                          • 0.12-0.13
                                                          • >0.13
Figure 5-33.  Second highest daily maximum (2HDM) for 1989 (A) and 1988 (B)
             estimated across crop growing regions in the eastern half of the country.
             2HDM interpolated across non-monitored regions based on the regression
             relationship with an exposure potential surface and monitored sties for
             those years.

Source:  Herstrom et al. (1993).
December 1993
                                     5-296      DRAFT-DO NOT QUOTE OR CITE

-------
         A. (1989)
                                                         Percent
                                                         Crop Loss
                                                         E3 0-10
                                                         m 11-20
                                                         • 21-30
                                                         • >30
         B. (1988)
                                                         Percent
                                                         Crop Loss
                                                         EZ 0-10
                                                         m 11-20
                                                         • 21-30
                                                            >30
Figure 5-34.  Estimated relative yield loss (ERYL) for all crops from NCLAN database
            across crop growing regions of the eastern half of the United States in
            1989 (A) and 1988 (B). Estimated relative yeild loss calculated for each
            20 km cell based on estimated ozone exposure value (3-mo SUM06) and
            Weibull parameters for all species' response function.


Source: Tingey et al. (1991).
December 1993
5-297     DRAFT-DO NOT QUOTE OR CITE

-------
       A. (1989).
                                                         Percent
                                                         Crop Loss
                                                             0-10
                                                             11-20
                                                             21-30
                                                             >30
        B. (1988)_
                                                         Percent
                                                         Crop Loss
                                                            0-10
                                                            11-20
                                                            21-30
                                                            >30
Figure 5-35.  Estimated relative yield loss (ERYL) in 1988 for soybean (A) and wheat
            from NCLAN database across crop growing regions of the eastern half of
            the United States in 1989 (A) and 1988 (B). Estimated relative yield loss
            calculated for each 20 km cell based on estimated ozone exposure value
            (3-mo SUM06) and Weibull parameters for all species response function.
December 1993
5-298
DRAFT-DO NOT QUOTE OR CITE

-------
  A. Aspen (1988)
     B. Aspen (1989)
December 1993
species response function.



                 5-299
                                       DRAFT-DO NOT QIXOT OR CITE

-------
             A. Black Cherry
             B. Red Maple
Figure 5-37.  Estimated biomass reduction (EBR) for black cherry (A) and red maple
            (B) with 1988 ozone exposure. Estimated biomass reduction calculated for
            each 20 km cell based on estimated ozone exposure value (3-mo SUM06)
            and Weibull parameters for each species response function. Note the
            different scales for the two species.  The EBR ranges from <20 to >30%
            in black cherry,  but red in maple,  EBR is < 2 to > 4% over its entire
            range.
December 1993
5-300
DRAFT-DO NOT QUOTE OR CITE

-------
             A. Loblolly Pine
             B. White Pine
Figure 5-38. Estimated relative biomass reduction (ERBR) for loblolly pine (A) and
            eastern white pine (B) with 1988 ozone exposure.  Estimated relative
            biomass reduction calculated for each 20 km cell based on estimated ozone
            exposure value (3-mo SUM06) and Weibull parameters for each species
            response function.  Note the scale difference for the two species.  Loblolly
            pine ranges from < 3 to > 6% ERBR, and eastern white pine range from
            <10to
December 1993
5-301
DRAFT-DO NOT QUOTE OR CITE

-------
 1     of a species is shown in Figure 5-36, using wild populations of trembling aspen seedling
 2     estimated total biomass reduction.  Species-dependent variation in response to O3 is
 3     illustrated in Figure 5-37.  A vast difference in exposure-response is observed between two
 4     species that occupy the same area geographically, black cherry and red maple.  Red maple,
 5     even in the high O3 year of 1988, is relatively insensitive compared to black cherry.  Red
 6     maple shows less than 2%  reduction in growth across its range, whereas black cherry shows
 7     a large portion of its range experiencing greater than 30% annual biomass reduction.  Pine
 8     species of the eastern U.S. also exhibit a difference in response to O3. Loblolly pine and
 9     eastern white pine are shown in Figure 5-38 for 1988. Only a small portion of the range of
10     loblolly pine is estimated to have greater than 2% reduction in total biomass, and eastern
11     white pine is estimated to have total  biomass reduction greater than  10% over more than half
12     of its range.
13          The range of estimated yield reduction for each of the crop species (Figure 5-39) and
14     the estimated annual total biomass reduction for each of the tree seedling species
15     (Figure 5-40) across all the area (10th to 90th percentile) is variable depending on  the species
16     and year. Corn is the least, ranging from 1 to 20%, and wheat has the widest range from
17     2 to 80% yield reduction.  The median (50% of the range) estimated yield reduction across
18     all  crop growing  areas is 18.9% in 1988 and only 3.1 % in 1989  illustrating the year-to-year
19     variation  in response.  The median for the four species indicates corn to be less sensitive and
20     wheat to be the most sensitive, based on area-weighted estimated yield reduction across the
21     area where the species are grown.
22          Tree species show a similar range of responses across their ranges.  A relatively small
23     range  in response is estimated across all the area of loblolly pine (4 to 7%) compared to
24     sugar  maple (0 to 50%) (Figure 5-40).  The median (50% of the range) annual biomass
25     reduction across all species range from 0% in Virginia pine and red maple to 33% in the
26     sensitive aspen clone.  Based on the median value for each species, the relative sensitivity of
27     seedlings based on area-weighted annual biomass reduction in  relation to estimated 1988
28     exposures are:  (1) Sensitive:  Aspen and black cherry with annual growth reductions of
29      14 to  33%; (2) Moderately Sensitive:  tulip poplar, loblolly pine, eastern white pine, and
30     sugar  maple having reductions of 5 to 13%; and  (3) Insensitive: Virginia pine and red maple
        December 1993                           5-302      DRAFT-DO NOT QUOTE OR CITE

-------
                                   Eastern United States 1988
                     100
                      80

                      60
                      40
                      20
i
  I


=
                                     -
4-
B
                              All
                                     Com
               Cotton    Soybean    Wheat
                                   Eastern United States 1989
100
^r so
1 80
c
8 40
1 20
1
0.
0



I

\ •• \
il * i i -

                              All     Com     Cotton    Soybean    Wheat

Figure 5-39.  Box-plots of annual area-weighted yield reduction for the four major
             agronomic crop species and all crops from NCLAN with estimated 1988
             (A) and 1989 (B) ozone exposure. The estimated yield reduction is taken
             from each 20 km cell in the species' distribution, weighted for area and
             the distribution plotted showing 10th (bracket), 25th (lower shaded box),
             50th (clear bar in shaded box), 75th (upper shaded box), and 90th
             (bracket) percentile.  The single values outside these percentiles are also
             plotted (closed circles). The percentiles represent the area of the species
             exhibiting that  level or less of yield reduction.
December 1993
          5-303
     DRAFT-DO NOT QUOTE OR CITE

-------
                
-------
 1      having losses of 0 to 1 % per year.  The biomass losses for 1989 are significantly less
 2      (Hogsett etal., 1994).
 3           There are uncertainties attached to these estimates, including:  (1) the estimations of
 4     O3 exposure in non-monitored areas; (2) the exposure-response functions for each species;
 5      (3) the climate and meteorological data; and (4) the accuracy of species distribution and the
 6     lack of any species density data.  This  listing is a rough order  of significance, although it
 7     would be difficult to distinguish between the first two.  In addition to the variation about the
 8     exposure-response function itself, there is the critical issue of the response function being
 9     developed from seedlings and under optimal growing conditions.  As such they probably do
10     not reflect mature tree response, and certainly do not reflect the response of species within
11      an ecosystem context.  But the  estimated biomass loss is a potential risk that species may
12     experience at least for seedling establishment,  reforestation or  natural regeneration.  Again,
13     the interactions that define a community response or an ecosystem  response are not included
14     in these spatial estimates.
15
16     5.9.11  What Is the  Effect of Ozone on  Ecosystems?
17          Most of the information dealing with the responses of ecosystems to 63 stress is based
18     on the study of the San Bernardino Forest ecosystem.
19          The mixed conifer  forest ecosystem in the San Bernardino Mountains of southern
20     California is one of the most thoroughly studied  ecosystems in the United States.  Chronic
21      O3 exposures over a period of 50 or more years  produced major changes in the San
22     Bernardino National Forest ecosystem.  The primary effect was on the more susceptible
23     members of the forest community, individuals of ponderosa and Jeffrey pine, in that they
24     were no longer able to compete effectively for essential nutrients, water,  light and  space.
25     As a consequence of altered competitive conditions in the  community, there was a  decline in
26     the sensitive species, permitting the enhanced growth of more  tolerant species (Miller et al.,
27     1982; U.S. Environmental Protection Agency, 1978, 1986). The results  of the studies of the
28     San Bernardino Forest ecosystem were reported  in both the 1978 and 1986 criteria
29     documents (U.S Environmental Protection Agency, 1978,  1986).
30          Ecosystem responses  to stress are hierarchical. They begin with the response of the
31      most sensitive individuals of a population.  Therefore, the response of an ecosystem to O3 is

       December 1993                          5-305      DRAFT-DO NOT QUOTE OR CITE

-------
 1      determined by how the responses of its most sensitive individuals affect the population.
 2      Foliar injury is usually the first visible indication of O3 exposure.  Stresses,  the primary
 3      effects of which occur at the molecular level of the individual, must be propagated
 4      progressively up through more integrated levels of organ physiology (e.g., leaf, branch, root)
 5      to whole plant physiology, to stand dynamics, and then to the landscape level to produce
 6      ecosystem effects (Hinckley et al.,  1992).  This is particularly true if the stress is of low-
 7      level because only a small fraction of stresses at the molecular level become disturbances at
 8      tree, stand, or landscape level.  Insect defoliation,  for example, may severely reduce the
 9      growth of one or several branches while growth of the tree appears not to be affected
10      (Hinckley  et al., 1993).  The time required for a stress to  be propagated from one level to
11      the next determines how soon the effects of the stress can  be observed or measured.
12      Therefore, to understand the effects of a stress, one must utilize a framework of hierarchical
13      scales (Figure 5-24; Section 5.7) such as that developed to provide a means  for following and
14      understanding the effects of the eruption of St. Helens on forest trees  (Hinckley et al., 1992).
15           The effect a stress at one hierarchial  level will have on a higher level are determined  by
16      variability and compensation.  Variability in response to stress may mean that, because of
17      genetic variation,  not all trees are equally  susceptible as was observed not only in the case  of
18      the sensitive ponderosa and Jeffrey pine in the San Bernardino Forest but also was true of the
19      eastern white pine in the Appalachian Mountains.   In both instances, trees were designated
20      sensitive, intermediate and tolerant.  At the stand  level, the slower growth of some trees may
21      be compensated for by the relatively faster growth of others that are experiencing reduced
22      competition so that the overall growth of the stand is not affected (Hinkley et al., 1992).
23      These properties,  when taken together, will determine the extent and rate at which stress at
24      one hierarchical level will impact the next highest level.  The stand level was affected in the
25      San Bernardino Forest but was not apparent in the Appalachian Mountains.  Figure 5-24
26      (Section 5.7), therefore, is also applicable for considering  the effects of O3 on forest stands
27      and can be used to help explain the difference between the response of the San Bernardino
28      Forest ecosystem  and the forest ecosystems in the eastern  United States.  As pointed out
29      above, variability and compensation determine the severity of the response of the individual
30      and the  length of time required for it to be expressed structurally and functionally.
        December 1993                           5-306       DRAFT-DO NOT QUOTE OR CITE

-------
  1           Variability and compensation can also occur at the population level, all populations do
  2      not respond equally but are influenced by the number of sensitive individuals (Taylor and
  3      Pitelka, 1992). Plant populations can respond in four different ways:  (1) no response, the
  4      individuals are resistant to  the stress;  (2) mortality of all individuals and local extinction of
  5      the extremely sensitive population—the most severe response;  (3) physiological
  6      accommodation, growth, and reproductive success of unaffected individuals because the
  7      stress is accommodated physiologically; and (4)  differential response, members of the
  8      population respond differentially with some individuals exhibiting better growth and
  9      reproductive success due to genetically determined traits (Taylor and Pitelka, 1992).
 10      Differential response results in the progressive elimination over several generations of the
 11      sensitive individuals and a  shift in the genetic structure of the population toward greater
 12      resistance (microevolution). Physiological accommodation or microevolution, with only the
 13      latter affecting biodiversity, are the most likely responses for exposure to chronic stress (i.e.,
 14      stresses that are of intermediate-to-low intensity  and of prolonged duration).  The primary
 15      effect of O3 on the more susceptible members of the plant community is that the plants can
 16      no longer compete effectively  for essential nutrients, water, light, and space and are
 17      eliminated.  The extent  of change that can occur in a community depends on the condition
 18      and type of community, as well as the exposure  (Garner, 1993).  Forest stands differ greatly
 19      in age, species composition, stability,  and capacity to recover from disturbance. For this
 20      reason, data dealing with the responses of one forest type may not be applicable to another
 21      forest type (Kozlowski,  1980).
 22           The factors explaining ecosystem responses at both the individual species and
 23      population level discussed above can be used to  explain why the San Bernardino Forest
 24      ecosystem has suffered more severe injury than ecosystems such as those in the Appalachian
 25      Mountains and in other  parts of the United States.   Changes in ecosystems begin with the
 26      death of individual plants.  Major changes in the San Bernardino ecosystem began with
 27      injury to ponderosa and Jeffrey pine.  Ecosystem responses,  therefore, began with the
 28      biochemical changes in the leaves of sensitive individuals and were transferred ultimately to
 29      the whole ecosystem.  Individuals of ponderosa pine were most sensitive to O3 exposure,
 30      with Jeffrey pine, white fir, black oak, incense cedar, and sugar pine  following in  decreasing
31      order.  Foliar injury on  sensitive ponderosa and  Jeffrey pine was observed when

        December 1993                           5.307      DRAFT-DO NOT QUOTE OR CITE

-------
 1     24-h-average O3 concentrations were 0.05 to 0.06 ppm (Miller et al., 1982). Structural
 2     changes within ecosystems are the result of functional changes that began within the
 3     individuals and were propagated to populations and to the community and then to the
 4     ecosystem (e.g., altering of nutrient cycling Miller et al., 1982).  Biochemical changes
 5     within the trees resulting from O3 exposure that were not repaired or compensated for were
 6     expressed as:  (1) visible foliar injury; (2) premature needle senescence; (3) reduced
 7     photosynthesis; (4)  reduced carbohydrate production and allocation; (5) reduced plant vigor;
 8     and (6) reduced growth or reproduction or both (Miller et al., 1982). These changes at the
 9     individual plant level lead to reduced  root growth, and reduced yields of fruits and seeds or
10     both, and change in competitive ability or reduced plant vigor.  Subsequently, they were
11     manifested as changes  in plant populations and communities and ultimately ecosystems.
12           In addition, the functional changes lead not only to injury to or changes in the
13     functioning of other living ecosystem  components, either directly or  indirectly, by altering
14     the processes  of carbon (energy)  flow and mineral nutrient cycling, water movement and
15     changed vegetational community  patterns (Miller et al., 1982).  Change in decomposition
16     patterns, the result  of early leaf senescence and changed successional patterns of leaf
17     microflora, altered  nutrient cycling.  Carbon and mineral nutrients accumulated in the heavy
18     and thick needle layers.  Biotic interactions associated with predators (insect pests),
19     pathogens (fungi), and symbionts (mycorrhizae) were altered by loss of tree vigor. In stands
20     with  a high proportion of O3-injured trees, a given population of western pine beetles could,
21     therefore, kill more trees.  The root rot fungus (Heterobasidium annosum) increased more
22     rapidly because freshly cut stumps of weakened trees were more vulnerable to attack (U.S.
23     Environmental Protection Agency, 1976,  1986).  The continuum of changes (Table 5-31;
24     Section 5.7)  beginning with injury to the individual trees resulted finally in  ecosystem
25     breakdown.  A shift in dominance from ponderosa and Jeffrey pine to Cytolerant shrub and
26     oak species was observed.
27           In the San Bernardino Mountains of California, O3 concentrations greater than
28     0.08 ppm for 1300 h,  with concentrations  rarely decreasing below 0.05 ppm at night near the
29      crest of the mountain slopes, have been observed over a period of 10 to 20 years.
30           Injury to sensitive vegetation in California continues to occur.  To date, such injury has
31      not resulted  in as extensive ecosystem change.

        December 1993                           5-308       DRAFT-DO NOT QUOTE OR CITE

-------
  1           Ozone-induced injury to vegetation has also been observed on the Cumberland Plateau
  2      in the eastern United States. In a study of 25-year old white pine, a reduction of 70% was
  3      observed over a 17-year period, when annual growth in diameter of sensitive trees was
  4      compared with that of intermediate and tolerant trees (McLauglin, 1982). Maximum 1-h
  5      O3 concentrations ranged from 0.12 to 0.3 ppm for the years  1975 through 1979. Decline in
  6      vigor and reduced growth was associated with premature senescence,  a loss of older needles
  7      and a reduction in photosynthesis.
  8           In the Appalachian Mountains, monthly 8-h average O3 concentrations ranging from
  9      0.35 to 0.65 ppm with peak hourly concentrations from 0.08 to 0.13 ppm caused foliar
10      injury, growth reductions and death of sensitive eastern white pine and growth reductions of
11      other indigenous forest tree species.
12           Despite the injury to the sensitive eastern white pine which resulted in a decline in
13      vigor and growth, the injury was apparently not severe enough to  be propagated to the stand
14      or ecosystem levels, except for possibly on  Mt. Mitchell,  NC.  On Mt. Mitchell the death of
15      Fraser fir and red spruce have also been attributed to the balsam wooly adelgid.  Therefore,
16      the extensive injury observed in the San Bernardino Mountains has not been observed in the
17      Appalachian Mountains.
18           Preliminary studies suggest that a nitrogen deposition gradient coincident with the
19      O3 gradient in the San Bernardino Mountains may play an important interactive role in forest
20      tree response.
21           The fact that changes in carbohydrate  allocation from the leaves to the roots in the
22      ponderosa, Jeffrey  and eastern white pine can alter the process wherein fungi and plant roots
23      form an important symbiotic relationship (mycorrhizae) has been mentioned.  These
24      relationships between plant roots and fungi are critical for both. Fungi take up minerals
25      (e.g., nitrogen) and make it available to plants for their use.  Plants, on the other hand,
26      through  their roots  supply  the fungi with energy (sugars) for their  growth.  Without the
27      nutrients, particularly nitrogen  which is critical in the process of photosynthesis, trees are
28      more vulnerable to abiotic stresses such as resulting from O3 exposure and to insect pests and
29      pathogens.
30
31

        December 1993                           5.399      DRAFT-DO NOT QUOTE OR CITE

-------
 1     5.9.12  Economic Assessments
 2          Based on economic assessments and scientific data available at the time, the previous
 3     criteria document (U.S. Environmental Protection Agency, 1986) concluded that O3 at
 4     ambient levels was imposing economic costs on society.  The review of more recent (post-
 5     1986) literature on agriculture corroborates that earlier conclusion.  Specifically, the recent
 6     literature, using the full set of NCLAN data and addressing some deficiencies in the pre-1986
 7     assessments, confirms the finding of economic losses from ambient O3 concentrations.
 8          The exact level of these economic effects is a function of cropping patterns,
 9     03 concentrations (both ambient and episodic), and the spatial and temporal characteristics of
10     projected or observed O3 levels. The current economic assessments represent improvements
11     in the scientific understanding of O3 effects on agriculture.  However, the assessments of
12     economic effects initially incident on the agricultural sector remains incomplete.
13          Only a few assessments consider the economic effects of 03 on forest trees as well as
14     urban trees, shrubs, and ornamentals.  These studies assess the economic effects of
15     hypothetical changes resulting from O3 or other stressors on forest productivity and aesthetics
16     and are best viewed as measures of the potential effect of O3 on these receptors.
17     Improvements linking O3 effects data to productivity and aesthetic effects will improve the
18     utility of such economic analyses.
19          The effects of O3 on ecosystems have not been addressed in the published literature.
20     There is, however, an emerging interest in applying economic concepts and methods to the
21     management of ecosystems.  Ecological research is also addressing the challenging
22     conceptual and practical issues in understanding and managing ecosystem functions.
23     Economic research continues to develop,  refine, and apply techniques for valuing market and
24     nonmarket products and services that will be of help in estimating the economic  effects of 03
25     on ecosystems. Increased dialogue between the disciplines is needed before empirical
26     analyses of the economic consequences of ecosystem management are feasible.
27          In summary, the state of science concerning O3 economic effects on agricultural crops
28     is sufficient to conclude that O3  imposes costs on society.
29
        December 1993                          5-310      DRAFT-DO NOT QUOTE OR CITE

-------
 1     5.10 EFFECTS OF OZONE ON MATERIALS
 2     5.10.1  Introduction
 3          Photochemical oxidants are capable of reacting with a number of man-made and natural
 4     materials.  Nearly all materials damage  research on photochemical oxidants has focused on
 5     economically important or abundant materials that are susceptible to oxidant damage. These
 6     include elastomers  (natural rubber and certain synthetic polymers), textile fibers and dyes,
 7     and, to a lesser extent, paints.  Recent research has been conducted on culturally important
 8     materials,  such as artists' paints and pigments. It has been shown that oxidants harden and
 9     embrittle elastomers, causing cracking and a loss in physical integrity.  Oxidant exposure
10     weakens certain textile fibers (i.e., reduces the breaking strength and increases the rate of
11     wear) and changes the color of some dyes.  The effects of oxidants on paints are not defined
12     well, but they may be similar to some of the effects on elastomers; damage from other
13     gaseous pollutants, such as sulfur dioxide and from natural damaging agents such as sunlight,
14     moisture,  oxygen, and temperature fluctuations tend to overshadow the role of ambient O3 in
15     causing  paint damage.
16          The  literature selected for review in this section includes research previously reported
17     in the 1978 and 1986 criteria documents (U.S. Environmental Protection Agency, 1978,
18     1986) and a limited number of other references published before and after 1986. Because
19     little recent work has been reported on the effects on materials, reference to older studies is
20     necessary  for unity and coherence.  This assessment of the effects on materials includes a
21     review of the mechanisms of damage and protection; it also presents dose-response
22     information from laboratory and field studies and evaluates previously reported economic
23     assessments.
24
25     5.10.2  Mechanisms of Ozone  Attack and Antiozonant Protection
26     5.10.2.1  Elastomers
27          Most elastomeric materials found in the marketplace are composed of unsaturated, long-
28     chain organic molecules.  That is, the molecules contain carbon-carbon double bonds.
29     Natural  rubber and synthetic polymers/copolymers of butadiene, isoprene,  and styrene
30     account for the bulk of elastomer production for products such as automobile tires (Mueller
31     and Stickney,  1970). These types of compounds are particularly susceptible to O3 attack.

       December 1993                          5-311      DRAFT-DO NOT QUOTE OR CITE

-------
 1     In contrast, synthetic elastomers with saturated chemical structures, such as butyl rubber,
 2     polymers of silicones, ethylene,  propylene, hypalon, and polyurethanes, have an inherent
 3     resistance to O3 damage, but higher cost and limiting physical and chemical properties have
 4     constrained their use in  outdoor  environments.
 5           Ozone is thought to attack  elastomers by adding a chain of three oxygen atoms directly
 6     across the double bond, forming a five-membered ring structure (Mueller and Stickney,
 7     1970).  This structure quickly rearranges (via Criegee ozonolysis) to form a zwitterion and
 8     an aldehyde (see Figure 5-41).  The aldehyde/zwitterion pair can be formed on either side of
 9     the point of chain scission.  Subsequent reactions of the zwitterion lead to a permanently
10     oxidized elastomer.  Ozone damage in  the form of cracking  is a surface phenomenon.  It is
11     greatly accelerated by mechanical stress, which produces fresh surface area at crack
12     boundaries. At very high concentrations and high  mechanical stress,  O3 damage can result in
13     a large number of surface microcracks  that produce a frosted appearance and mechanical
14     weakening (Crabtree and Malm, 1956). At pollutant concentrations normally encountered
15     outdoors (and in many indoor environments), the elastomer hardens or becomes brittle and
16     cracked, which results in a loss of physical integrity.
17           According to Fisher (1957), work at the Rock Island Arsenal by R.  F.  Shaw, Z.  T.
18     Ossefa and  W. J. Tonkey in  1954 led to the development of effective antioxidant additives to
19     protect elastomers from O3 degradation.  Subsequently, antiozonants were generally
20     incorporated into elastomeric formulations during mixing,  and their protection was effective
21     even when elastomers were stretched or flexed (Fisher, 1957; Mueller and Stickney, 1970).
22           Several theories (Andries and Diem, 1974) have been advanced to explain the
23     mechanism of antiozonant protection.  The two best supported theories are the scavenger
24     theory and the protective film theory.  The scavenger theory suggests that the antiozonant
25     diffuses  to the surface, where it reacts  with the O3 at a faster rate than with the
26     carbon-carbon double bonds of the rubber, thereby protecting the rubber sacrificially.  The
27     protective film theory also includes diffusion to the surface,  but assumes that the resulting
28     layer is  less reactive with O3 than is the rubber and thus constitutes a protective layer.
29           The work  of Razumovskii  and  Batashova (1970) on the mechanism of protective  action
30     by the antiozonant N-phenyl-N'-isopropyl-/?-phenylenediamine (PIPP) is most consistent with
        December 1993                           5-312      DRAFT-DO NOT QUOTE OR CITE

-------
c
H
                   H  H
                                                          O
                                                  R   O    O
   C   C   C —
   H   H   H
                                                                                     (a)
                     O
                   /  \
              R   O    O
              C
  ;—C—C
     H    H
             H
R
 t
 I
C
H
C   O   O + OC
H                  H
(b)
       Figure 5-41. Postulated mechanism for damage to elastomers by ozone.
       Source:  Mueller and Stickney (1970).

 1     the scavenger mechanism. These investigators showed that O3 reacts preferentially with
 2     PIPP at a ratio of three O3 molecules per one PIPP molecule.
 3          Andries et al.  (1979), using carbon-black-loaded natural rubber (NR) compounds with
 4     and without antiozonants, attempted to distinguish among possible mechanisms with
 5     attenuated total reflectance spectroscopy and scanning electron microscopy. Their
 6     experiments indicated that a combination of the scavenger and protective film mechanisms
 7     best explains antiozonant protection.  Examination of the surface of the rubber samples with
 8     antiozonant showed that only ozonized antioxidant and not ozonized rubber was present.
 9     This layer of ozonized antioxidant functioned as a relatively nonreactive film over the
10     surface, preventing  the O3 from reaching and reacting with the rubber below.
11          Lattimer et al. (1984) conducted a series of experiments on cross-linked rubber
12     (cw-polyisoprene and  cw-polybutadiene) containing N,N'-di-(l-methylheptyl)-/7-
13     phenylenediamine antiozonant.  They concluded that while a number of O3-rubber reactions
14     and mechanisms are possible, these  reactions do not become significant until the antiozonant
       December 1993
                                   5-313
            DRAFT-DO NOT QUOTE OR CITE

-------
 1     is nearly completely consumed (i.e., the antiozonant preferentially reacts with the O3).  They
 2     concluded that the "scavenger-protective film mechanism" is primarily responsible for
 3     antiozonant protection.
 4          In addition to reactive antiozonants, paraffinic and microcrystalline waxes are used to
 5     protect the elastomers in rubber products such as tires.  The wax migrates to the surface of
 6     the rubber and forms a barrier against O3 attack. Dimauro et al. (1979) studied the ability of
 7     18 waxes to protect rubber against degradation from O3. Dimauro found that no wax by
 8     itself provided an optimal level of protection; blending with a reactive antiozonant was
 9     required.  The paraffinic waxes protected best at lower exposure temperatures, and the
10     microcrystalline waxes were more effective at higher temperatures.  Wax blends,  which
11     combine the best effects of each type of wax,  offered  the best protection over a wide range
12     of temperature (Lake and Mente, 1992).  It was found,  however, that wax alone can be
13     detrimental to dynamic O3 resistance.  Wax can induce  localized stresses in the rubber  that
14     can lead to premature rubber failure under dynamic testing conditions.
15
16     5.10.2.2  Textile Fibers and Dyes
17          Cellulose-based fibers, acrylic fibers, and nylon  fibers are affected by O3 (Zeronian
18     et al.,  1971);  however,  it is difficult to distinguish O3-induced damage from oxidation by
19     molecular oxygen.  Reduction in breaking  strength and  an increased rate of wear are the
20     types of damage  most commonly observed. As stated by Bogaty et al. (1952), however, for
21     most uses of textile fibers the action of O3 is less important in affecting product lifetime than
22     physical abrasion, biological degradation,  soiling, fashion, and other factors.  Furthermore,
23     most textiles are used and spend  most of their life indoors where O3 concentrations are
24     usually less than outdoor O3 concentration (Yocom et al., 1986).  Accordingly, the economic
25      significance of O3  damage to textile fibers is relatively low, and the differences in the
26      mechanisms of attack are not important.
27           Many textile  dyes react with O3. Figure 5-42 illustrates the reaction of Disperse
28      Blue #3 with  O3 and with nitrogen oxides  (Haylock and Rush, 1976).  Ozone attacked the
29      quinoid portion of the molecule,  completely rupturing the ring system chromophore and
30      oxidizing the dye to phthalic acid,  which is colorless.  Matsui et al. (1988) investigated the
31      reactions of O3 with aromatic azo compounds.  Ozone was found to attack both the aromatic

        December 1993                           5-314      DRAFT-DO NOT QUOTE OR CITE

-------
                                 R
                           O   NH
                            i1
                           O
                                NH
                                 R
                                               Ozone
Nitrogen
  Oxides
                       O
                        II
                       C—OH
                       C—OH
                       0
              Disperse Blue No. 3
       Figure 5-42. Reaction of anthraquinone dyes with ozone and with nitrogen oxides.
       Source: Haylock and Rush (1976).

 1      rings and the more electron-rich nitrogen atoms.  Both the direct attack on the azo dye
 2      structure and the production of daughter products alter the original dye color.
 3           The reactions between various dyestuffs and O3 are influenced by the chemical nature
 4      of the fiber to which the dye is applied and the manner in which the dye is applied.
 5      Additional factors include the presence of protective agents; effects of temperature, air
 6      moisture, and other pollutants; and even the degree of strain of the base fiber caused by
 7      folding or creasing.  In a study of O3 fading of anthraquinone dyes on nylon, Haylock and
 8      Rush (1976, 1978) found that fiber properties such as cross-section shape, draw ratio, and
 9      the degree of steam heat setting had significant effects on the rate and severity of 63 damage,
10      even for chemically identical systems.  Moore et al. (1984) found that the rate of O3 fading
11      of acid and disperse dyes on polyamide fibers appeared to be a function of rate of dye
12      migration to the surface of the fibers.  Thus using dyes that diffuse slowly (high  molecular
13      weight dyes) improved resistance to O3 fading. Given this complexity and sensitivity for
       December 1993
5-315
DRAFT-DO NOT QUOTE OR CITE

-------
 1      both dye and fiber type, it is not possible to relate a specific mechanism of damage to a
 2      broad class of damage situations.
 3
 4      5.10.2.3 Paint
 5           The mechanisms of architectural paint and coil coating damage caused by O3 have not
 6      been well defined. Damage is probably related to oxidation of the organic binders that hold
 7      the pigment and form the protective seal over the surface.  Damage is likely to be similar to
 8      that of elastomers; that is, embrittlement and cracking as the result of chain scission and
 9      cross-Unking.  The data available on O3 damage to architectural paints, however, come
10      primarily from studies of surface erosion caused by gaseous pollutants, and the suspected
11      O3 damage patterns (embrittlement and cracking) are not quantified.  Because  the polymeric
12      structure of dried paint film is significantly different from that of an  elastomer under
13      elongation stress,  direct comparisons should be made with great caution.
14           In a series of experiments (Shaver et al., 1983;  Grosjean et al., 1987; Grosjean et al.,
15      1988a,b; Grosjean et al., 1989) the direct attack of O3 on artists' pigments and paints was
16      investigated. Ozone was found to react with alizarin pigments, indigoes, curcumin and
17      triphenylmethane  colorants.  The exact  mechanism and site of the attack (e.g., carbon-carbon
is      unsaturated  bonds, aromatic rings,  or carbon-nitrogen bonds) and subsequent reactions with
19      the daughter products depended on the  initial structure of the pigment.  Often  the products of
20      these reactions were  colorless or of a noticeably different color than  the original pigments,
21      resulting in  fading or color changes.
22
23      5.10.3  Exposure-Response Data
24           Laboratory exposure-response studies are criticized for their reliance on artificial
25      environments that do not contain all the critical variables encountered under ambient
26      conditions.  Scientists realize the limitations of laboratory tests; no model could simulate
27      conditions identical to an ambient environment. Nevertheless,  many laboratory tests have
28     represented the outdoor environment to some extent,  and the findings from these tests have
29     been used in conjunction with field tests to estimate the nature and amount of  damage to
30     materials.  Controlled field tests have the advantage of being carried out under real exposure
       December 1993                          5-316      DRAFT-DO NOT QUOTE OR CITE

-------
 i      conditions, but, because of the highly variable nature of real exposure conditions, data
 2      interpretation is difficult.
 3
 4      5.10.3.1 Elastomer Cracking
 5           Table 5-35 presents an overview of the available laboratory and field studies of the
 6      effects of O3 on elastomers.  Hofmann and Miller (1969) demonstrated correlations between
 7      laboratory tests and the actual service use of passenger vehicle tires in the Los Angeles area.
 8      Basically, three laboratory test methods were used: indoor and outdoor belt flex, indoor and
 9      outdoor wheel, and stress relaxation.  They found that the behavior of rubber exposed to
10      O3 under laboratory conditions correlated well with the service  behavior of tires in localities
11      where atmospheric O3 concentrations were high.
12           Bradley and Haagen-Smit (1951) evaluated a natural rubber (NR) formulation for
13      susceptibility to O3 cracking.  Strips were strained approximately 100% by bending and then
14      exposed in a small chamber to 20,000 ppm of O3; these specimens cracked almost
15      instantaneously and broke completely within 1 s.  When these NR formulations were exposed
16      to lower concentrations of O3 (approximately 0.02 to 0.46 ppm) time periods  of about 5 min
17      to over an hour were required for cracks to develop.
is           Meyer and Sommer (1957) exposed thin polybutadiene specimens to constant  load,
19      ambient room  air, and O3.  Specimens exposed in the summer to average O3  concentrations
20      of about 0.048 ppm broke after 150 to 250 h. In the fall, at average O3  concentrations of
21      0.042 ppm, specimens failed after exposures of 400 to 500 h. In the winter,  at average
22      O3 concentrations of 0.024 ppm, failures occurred between 500 and 700 h. These  data show
23      the strong dependence of breakage on O3 dose over the average time of exposure at which
24      failure occurred (average concentrations  x time).
25           Edwards and Storey (1959) presented data demonstrating the O3 resistance of two
26      styrene-butadiene rubber (SBR) compounds (Polysar S and Polysar Krylene).  Both
27      compounds were exposed without and with different levels of antiozonant protection to
28      0.25 ± 0.05 ppm of O3 at 120 °F (49 °C) under 100% strain (twice the  original sample
29      length).  Without antiozonants, a linear relationship was found between O3  dose (ppm-h) and
30      cracking depth.  Increasing the amount of antiozonants significantly reduced the rate of
31      cracking for both rubber compounds in a dose-related manner.

       December 1993                           5-317     DRAFT-DO NOT QUOTE OR CITE

-------
          TABLE 5-35. LABORATORY AND FIELD STUDIES ON EFFECTS OF OZONE ON ELASTOMERS
1 ====
O* Conditions
i—1 Laboratory/
VO f , j
^0 field
U)







Laboratory



Field
i
^
oo
Laboratory


O
"?>
2 Laboratory
i
5
o
25
g
H
/O Laboratory
CJ
9
a
o
Material/ Concentration
Product Pollutant ppm
Automotive Ozone 0.25 to 0.5
tires



Ambient air 0.04
(annual
average)


Vulcanized Ozone 0.02 to 0.46.
rubber strips 20,000


Rubber tires Ambient air 0.023 to
and various 0.048
polymers

SBR: PlysarS Ozone 0.25
Plysar Krylene
with and without
antiozonants

White sidewall Ozone 0.05 to 0.5
tire specimens





Polyisoprene Ozone 0 to 1.8




, Environmental Dose,
Exposure Variables ppm-h Effects
NA Tires under stress — Cracking of white
side wall.



> 1 year Los Angeles > 350 Positive
environment; correlation
actual service use between
laboratory and
ambient air tests.
3 to 65 min Physical stress -0.02 to 0.03 Surface cracking.



150 to 700 h Physical stress 9 to 20 Time of cracking
and ambient
environment

19 to 51 h 120 °F, 4.75 to 12 75 Percent
100% strain antiozonant was
related
to cracking depth
rate.
250 to 1,000 h 10 and 20% strain 20 to 500 Mean cracking
rates were
determined for
different stress
and 03 levels.


2 h 22 °C Up to 3.6 Cracking, stress
relaxation




Comment
Purpose was to correlate lab
and field tests. Exposure
time, detailed pollutant
measurements, and statistical
analyses were not reported.





Test was designed to establish
dose/response curves on
Oj-sensitive rubber for use an
analytical method.
Cracking occurred over a
broad range of values and
was related to stress.

Demonstrated dose/ response
linear relationship for O3 on
unprotected rubber.


Detailed data not available to
verify author's statement that
2 to .5 years of ambient
conditions were required for
03 cracks to penetrate cord
depth.

Rate of attack rapid and
proportional to
03 concentration



Reference
Hoffman and
Miller (1969)








Bradley and
Haagen-Smit
(1951)

Meyer and
Sommer (1957)


Edwards and
Storey (1959)



Haynie et al.
(1976)





Razumovskii
et al. (1988)



n

-------
       TABLE 5-35 (cont'd). LABORATORY AND FIELD STUDIES ON EFFECTS OF OZONE ON ELASTOMERS
1 ====
O* Conditions
, . Laboratory


Laboratory
Laboratory
Laboratory
UJ
O
6
o
25
9
1
S
O
Material/
Product Pollutant
Ten different NR, Ozone
SBR, CR
formulations with
and without
protection
Natural rubber, Ozone
epoxidised rubber,
copolymers
Several NR/SBR Ozone
blends with and
without protection
Tire cords Ozone
(66 nylon; Dacron
polyester; Kevlar
aramid)





Concentration, Environmental Dose,
ppm Exposure Variables ppm-h Effects Comment
0.5 Up to 300 h 30 °C Up to 50 Time to 10 to 20% Both formulation and
relaxation protection affected
relaxation.


0.05 to 1,000 to!6h -20 to 70 °C, 0 to 240 Time to first cracking Temperature
10 to 100% strain dependence of
antiozonant protection.
0.05 to 015 ~3tol6h Sunlight, -0.15 to 2. 4 Interply adhesion Both waxes and
humidity affected at 0.05 ppm and antiozonants needed for
above. protection against
sunlight plus 03.
0 to 1 5 0 to 48 h UV light; heat Up to 72 RFL adhesion loss Synergism between O3
(100 °C); RH (20 occurred primarily and RH; RFL
to 90%); NO-) during 6 h exposure to deterioration occurred
high RH and 0.2 ppm at surface.
Oj.





Reference
Ganslandt and
Svensson
(1980)


Lake and
Mente (1992)
Davies(1979)
Wenghoeter
(1974)





n

-------
 1          Haynie et al. (1976) conducted a chamber study to evaluate the effects of various
 2     pollutants, including O3,  on several materials.  In one part of the study, white sidewall
 3     specimens from a top-quality, steel-belted radial tire were exposed  (strained at 10 and 20%)
 4     for 250, 500, and 1,000 h to O3 concentrations of 0.082 ppm (160 /*g/m3) and 0.5 ppm
                   3
 5     (1,000 ji*g/m ). The O3 level was found to be statistically significant in the rate of cracking
 6     of this rubber.  However, cracking rates were not directly proportional to O3 concentrations
 7     for these two levels. Using the mean cracking rate calculated after long-term (1,000 h)
 8     exposure to conditions  representative of the primary air quality  standard for O3 and the
 9     annual average standard for nitrogen dioxide (NO2), Haynie et al. (1976) concluded that it
10     would take a minimum of 2.5 years for a crack to penetrate to the  cord depth. For this
11     particular premium  tire, therefore, sidewall failure from O3 damage does not appear to be the
12     cause of reduced tire life. Tread wear, rather than sidewall failure, probably determines the
13     life of a typical rubber tire.
14          Razumovskii et al. (1988) studied the decrease in  stress (stress relaxation) of
15     polyisoprene vulcanizates in an  exposure chamber at 22 °C at five O3 concentrations ranging
16     from O3 free to 3,450 /*g/m3 (1.76 ppm).  Stress relaxation resulting from the growth of
17     surface cracks caused irreversible changes in the dimension of the elastomer and decreased
18     tensile strength. Figure 5-43 presents  the rate of change of stress as a function of time for
19     various O3 concentrations.  The rate of stress reduction was proportional to
20     O3 concentration, with virtually no change for the O3-free  samples and progressively more
21     rapid relaxation as O3 levels increased.  Razumovskii et al. (1988) concluded that
22     O3 absorption,  attack of the C=C bonds, cracking and  resulting stress relaxation were fast
23     processes for unprotected elastomers.
24          Ganslandt and Svensson (1980) tested 10 different mixtures of three rubber compounds,
25     NR, SBR, and CR (a compound not defined  by the authors), with the isoelastic force
26     method.  The O3 protection afforded each rubber formulation is summarized in Table 5-36.
27     The samples at 50% elongation were exposed to O3 concentrations of 0.5 ppm at 30 °C.
28     The time to 10 and 20%  relaxation of the isoelastic force in the rubber test samples was used
29     to gauge the O3 resistance of the formulation.  Compounds GL 2073 B, SS 202, and
30     SS 200 C showed greatest resistance to the effects of O3, and those formulations that were
31     unprotected (GL 2073  D, SS 200 B, SS 202  A, SS 202) and the formulations protected only

       December 1993                          5,320      DRAFT-DO NOT QUOTE OR CITE

-------
                                       60   75    90   105   120
                                        t (min)
Figure 5-43.  Relative decrease in stress with time as a function of ozone concentration
             for polyisoprene vulcanizate.

Source: Razumovskii et al. (1988).
         TABLE 5-36. PROTECTION OF TESTED RUBBER MATERIALS
Protected
Rubber Formulation
GL 2073


SS 200

SS202

SS203

B, C
G
D
A, C
B
A
B

Unprotected


X

X
X

X
Wax
X
X

X


X

Antiozonant
X


X


X

Source: Ganslandt and Svensson (1980).
December 1993
5-321      DRAFT-DO NOT QUOTE OR CITE

-------
 1     by paraffin wax (GL 2073 G) demonstrated the least resistance to O3 attack. The testing
 2     showed great variety in the kinds of visible cracking effects as a result of the exposure. The
 3     compounds with no  protection often showed a large number of small cracks over the entire
 4     surface of the material, but those compounds protected by a combination of wax and
 5     antiozonant or by  wax alone sometimes showed only a single crack, which grew rapidly.
 6     These effects are demonstrated in Figure 5-44. Compounds SS 202 B (Figure 5-44a) and
 7     SS 200 C (Figure 5-44b), both protected with wax and antiozonant,  showed fairly good
 8     resistance when gauged by the 10 and 20% stress relaxation tests but failed after
 9     approximately 50  h  and 58 h of exposure,  respectively.  On the other hand, compounds
10     SS 203 and SS 200  B, both unprotected, exhibited small surface cracking and outlasted some
11     of the protected compounds.  Moreover, protection with wax and antiozonant may afford
12     long-term protection, but when one crack appears, it can grow rapidly and cut off the test
13     piece, as shown in Figure 5-44b.
14          Lake and Mente  (1992) exposed natural  rubber, epoxidised rubber and two
15     acrylonitrile-butadiene copolymers with chemical antioxidants, waxes or a combination of
16     antioxidants and waxes to a variety of O3 concentrations and  temperatures in environmental
17     testing enclosures.  Ozone concentrations ranged from 0.05 ppm to 1,000 ppm with
18     temperatures from —20 to 70 °C. Samples were kept under  constant strain between 10%
19     and 100%.  Antiozonant chemicals in the concentration range from 2 to 20 p.h.r. (parts per
20     hundred of rubber by weight) were tested and wax/antiozonant combinations at 6 p.h.r. wax
21     and 3 p.h.r. antiozonant were also tested.  Lake and Mente found that O3 protection was
22     most effective at higher temperatures, when diffusion of the antiozonant and wax to the
23     surface of the elastomers was most rapid.  This relationship is fortunate as ambient
24     O3 concentrations correlate well with higher temperatures.  Antiozonants became generally
25     less effective as temperatures dropped; however, dialkyl paraphenylenediamine provided
26     reasonable protection for natural rubber to  —17 °C.
27          Davies (1979)  reported on  the effects of O3 and other environmental factors on interply
28     adhesion of natural  and synthetic nibber compounds. Excellent adhesion of plies is essential
29     to the  proper manufacturing of tires.  The rubber strips must make interlocking contact at the
30     joint boundary or the strength of the tire will be inadequate.  Ozone attack  on synthetic poly
31     isoprene and polybutadiene produces a surface layer of ozonides.  With NR, the film consists

       December 1993                          5-322      DRAFT-DO NOT  QUOTE OR CITE

-------
            o
            o
.0
to
CO
                  100
             8     50
30

 0
                                                      CR (SS 203)
                         SBR Unprotected
                         (SS 202 A)

                        (a)
      SBR, Wax + Antiozonant
      (SS 202 B)

                     0   10  20  30  40  50  60  70  80  90 100
                                   Relaxation Time (h)
                                                     + Antiozonant
                                                 (Double Amount
                                                    mpared to A)
                     0   10  20  30  40  50  60 70  80  90 100

                                   Relaxation Time (h)

Figure 5-44.   Relaxation of rubber compounds in ozone is affected by the combination
             of rubber formulation and type of ozone protection. Compounds were
             tested at ozone concentration, 0.5 ppm; temperature, 30 °C; elongation,
             50%. Vertical line at the end of a curve means total failure, and vertical
             axis represents relaxation where FQ is the initial force and Ft is the force
             after time t.

Source: Ganslandt and Svensson (1980).
December 1993
5-323
                                  DRAFT-DO NOT QUOTE OR CITE

-------
 1     of ozonides and carbonyl groups (Andries and Diem, 1974; Andries et al., 1979).  The
 2     results of the Davies (1979) tests indicated that before curing, the adhesion of SBR
 3     compounds is unaffected by exposure to O3 concentrations of 0.15 ppm, but the adhesion of
 4     the NR/SBR blend decreases by approximately 30%. Large reductions (on the order of
 5     70%) in adhesion between plies were noted with the NR compounds; even exposure for a
 6     few hours at 0.05 ppm reduced adhesion considerably.  The adhesion tests on cured NR,
 7     SBR, and isoprene rubber (IR) compounds after exposure to various levels of O3 and
 8     humidity are summarized in Table 5-37.  The adhesion of the SBR compound is superior to
 9     that of the other two compounds, which were greatly affected by increased RH.
10
        TABLE 5-37. EFFECT OF OZONE AND HUMIDITY ON INTERPLY ADHESION3
Compound
NR
IR
SBR
Initial
Adhesion
5
5
5

0.15 ppm O3
(294 /ig/m3),
30% RH
2 to 3
4 to 5
4 to 5
Final Adhesionb
0.25 ppm O3
(490 /ig/m3),
30% RH
1
2tol
3 to 4

0.15 ppm O3
(294 ^g/m3),
60% RH
1
1
3 to 4
        Adhesion is rated from 1 (bad) to 5 (excellent), based on visual scale standardized by the authors.
        All exposures were 16 h in duration.
       Source:  Adapted from Davies (1979).
 1          Wenghoefer (1974) studied the effects of O3 on adhesion of tire cords dipped in
 2     resorcinal-formaldehyde latex (RFL). Many fibers and dip formulations were studied to
 3     determine their sensitivity to O3, humidity, nitrogen dioxide (NO2), UV light, and heat.
 4     Wenghoefer exposed these materials at a constant temperature of 100 °F (37.8 °C) to
 5     O3 levels that varied between 0 and 1.5 ppm (0 and 2,940 ^g/m3) and to relative humidity
 6     (RH) levels ranging from  20 to 90%. Adhesion deteriorated from changes in surface
 7     properties of the RFL-dipped cords as a result of exposure to O3, humidity, UV light, and
 8     heat. The adhesion losses from O3 and the combined effects of O3 and humidity were  most


       December 1993                         5-324     DRAFT-DO NOT QUOTE OR CITE

-------
  1     notable in the first 6 h of exposure. The detrimental effects of heat, NC^, and the
  2     synergistic interaction of NO2 and humidity were much less pronounced.
  3
  4     5.10.3.2 Dye Fading
  5          Color fading of certain textile dyes has been attributed to the effects of ambient Qj.
  6     Although NO2 was originally identified as the pollutant most important to color fading, the
  7     effects of O3 were noted by Salvin and Walker (1955).  The primary products affected were
  8     permanent press garments  (polyester and cotton) and nylon carpeting. Table 5-38
  9     summarizes studies on the effects of ozone on dyes.  By using a combination of laboratory
 10     chamber studies and  outdoor exposures, Salvin and Walker (1955) demonstrated that O3 was
 11     responsible for  dye fading observed on drapery fabrics. Blue anthraquinone dyes and  certain
 12     red anthraquinone dyes were markedly bleached after exposure to just 0.1 ppm of O3.   Azo
 13     red and yellow  dyestuffs and diphenylamine yellow dyes were shown to be resistant to fading
 14     at these concentrations, also confirming the results of the field study.  The use of known
 15     antiozonants, such as diphenyl-ethylenediamine and diallyl phthalate, in combination with
 16     disperse blue dyes was effective against O3 fading, thus providing additional evidence  of the
 17     effects of O3 on dyed fabrics.
 18          Ajax et al. (1967) summarized the results of a study of 69 dye-fabric combinations that
 19     were exposed outdoors in light-free cabinets at  11  sites. These sites were Sarasota, Florida;
 20     Phoenix, Arizona; Cincinnati, Ohio; and four urban-rural combinations:   Chicago and
 21     Argonne, Illinois; Washington, D.C., and Poolesville, Maryland; Los Angeles and Santa
 22     Paula, California; and Tacoma and Purdy, Washington. Among those fabrics exhibiting a
 23     high degree of fading at  both urban and rural sites in the first 6 mo, fading was much  greater
 24     at the urban sites than at the rural sites. The samples exposed in Phoenix, Sarasota, and
 25     Purdy showed the lowest amount of fading, which indicated that humidity and temperature
26     are not, by  themselves, the primary factors in fading.  The highest fading rate occurred in
27     samples exposed in Los Angeles, Chicago, and Washington, D.C.  In addition, there was a
28     marked seasonal variation in the test results, with greater fading during the spring and
29     summer seasons.  Generally, the results correspond with seasonal peaks in O3 concentrations.
30         Ajax et al. (1967) also exposed the fabrics to irradiated and nonirradiated auto exhaust
31      with and without sulfur dioxide (SO2) for 9 h/day for six consecutive days.  From the  results

        December 1993                           5.325      DRAFT-DO NOT QUOTE OR CITE

-------


O
z

9
fa
g
0
§
§
S
0
fa
o
H
1
i
H
2
fa
O

^5

|
•••J
^
z



^"^
1
D
S
J
•
3O
i
«o
a
^
H





i
2
1




«0
O
U

1


1 „
vironmei
Variable!
W

3
o



a
o
•s
g 0
!i
a
o
U


_o
"a
tti








»
M
"3 §
^ C. p^
•2 -: &
§ " -
C»^^ D —
._- *O "

* *«H '^T "l>
W -^ < CO
w 2 « "
1 ^ -111 • 1 1 isrl i alfj ^§
lljljli !ii!l{[ jilpllli
llllllz< Ill^llI llfllllll
s',,- c'Sao . »o s««
1^1 aM £« 1II1JI. |!«
if ^ tfil li liiiS-^ili'-s^
fSli
fill
a538« £siDea§<2 £Ji2°^g-s8H cT^ 8
»
-£ S ^
"-O t- H O
« 3 N 2K
05 3 ^
2 • |S
£* § g.? u ii
."§ £ 2 1 ° ° S


•*= i "*
1 ^ fN
1 >n c^ OUOUc^^^^<3^ZZO^I
T3
'J
Z ~i • rlrl 1£ -"•*1|'2<2
"8 S-' ?'-" "3— -oc — vn»~ Tf £ « 3 3 9
C ^«o •c_"'_ HT)"uT?-a-'ou"H3c'333
73 aj^^Joaioia* "^ JlWol)8j>T3::-"o'^"3«»Oft
3 8-^ij— S-S-l-ll 8 • !§ 'I 8 ^3 3 3 •§ •§ .*3 g< §< §<
5 i5i5i!!Si555Qa: i5a:<«


jt p Q
| | 0
g- g-h
3 3 <
December 1993
5-326
DRAFT-DO NOT QUOTE OR CITE

-------
I
u>
          TABLE 5-38 (cont'd).  LABORATORY AND FIELD STUDIES OF THE EFFECTS OF OZONE ON DYE FADING
     Dye
                              Fabric
                                         Concentration
                                            (ppm)
                  Exposure
                                   Environmental
                                     Variables
                                                                                                             Effects
                                                                                                                               Comments
                                                                                    Reference
Olive I and II
Disperse blue
3 and?
                       Nylon fibers
                       Nylon fibers
0.2
0.9
1 to >6 h
RH = 70 to 90%
Temperature = 40 °C
Visible fading in Olive  Both RH and 03      Haylock and Rush
I after 16 h at 70% RH; concentration affected  (1976)
same effect after 4 h at  fading and in a nearly
90% RH.  Linear      linear fashion. Sleeve
increase in fading at 0.9 form was more
ppm 03.              susceptible than skein
                    form.  Haylock and
                    Rush (1976) found
                    that: (1) increased
                    fiber draw ratio
                    reduced fading;
                    (2) increased heat-
                    setting temperature
                    increased fading;
                    (3) increased fiber
                    surface area increased
                    fading.
     Disperse blue dye in  Nylon 6 yarn
     an avocado green
     mixture
                                                  0.5
                                                                            RH = 85%
                                                                            Temperature = 40 °C
                                                    Fading was closely     Insufficient data for
                                                    correlated with fiber    dose-response
                                                    surface area (diameter), relationship
                                                                        determinations.
                                                                                                                                             Huevel et al. (1978)
j_j 2 Disperse dyes and Nylon 6 and Nylon 66
M 2 acid dyes Carpet
M
"~l Disperse blue 3 Nylon 6 yarn
B'


2
0
H
O
3
3 mo to 3 years 28 homes in different Geographic and
parts of the country seasonal variation in
fading.
0.2 2 to 120 h RH = 65%, 85%, 90% Nearly linear increase
Temperature = 40 °C in fading with time.
RH had a major
influence on fading
rate.



Field study. Nipe (1981)


This study focused Kamath et al. (1983)
more on mechanisms
of 03 fading rather
than dose-response
relationships.




-------
TABLE 5-38 (cont'd). LABORATORY AND FIELD STUDIES OF THE EFFECTS OF OZONE ON DYE FADING
ST Dye
f» 	 • •
>— ' Disperse, basic
^§ Disperse
W Direct vat, sulfur,
fiber reactive
Disperse
Disperse, acid
Direct
Acid, mordant
Disperse blue 3
Acid blue 25
Acid blue 40
Acid blue 45
Acid blue 80
Acid blue 127
Royal blue
^ Red
^ Plum
N>
Concentration
Fabric (ppm) Exposure
Acrylic 2 years in 3-mo
Cellulose acetate blocks
Cotton
Polyester
Nylon
Viscose rayon
Wool
Nylon 6 yarn 0.2 0 to 96 h
Nylon 66 yarn
Drapery fabric 0.5 and 1 .0 250 - 1,000 h
Rayon acetate
Rayon acetate
Cotton duck
Environmental
Variables Effects Comments
Light-proof cabinets, Two-thirds of samples Field study.
8 rural and urban sites exhibited substantial
fading, O3 was
significant for
8 fabric/dye
combination.
RH = 85 % Fading proceeded Study of mechanisms
Temperature = 40 °C consistent with of 03 fading, follow-
diffusion of dye to fiber on the Kamath et al .
surface (1983).
50 and 90% RH, NO2 03 was not statistically Laboratory study.
and SOi. significant cause of
fading.
Reference
Beloin (1972)
Moore et al. (1 984)
Haynie et al. (1 976)
aCoupling component 2. azoic diazo component 32.
s
1
1
g

-------
  1      of this chamber study, they noted that "photochemically produced byproducts of automobile
  2      exhaust are a prime cause of fading compared to fading caused by nonirradiated auto exhaust
  3      or by clean air with sulfur dioxide added."  In the presence of SO2, however, a more than
  4      additive effect was seen in the dye fading tests for both chamber and field studies.  Although
  5      their conclusions concerning O3 itself are easily substantiated in the research literature, the
  6      O3 levels measured in their chamber are questionable.  The daily 9-h average
  7      O3 concentrations (measured by neutral KI,  Mast instrument) were identical for irradiated
  8      (UV) and nonirradiated exhaust (0.02 ppm); irradiated  exhaust plus SO2 produced 0.55 ppm
  9      of 03.
10          Beloin (1972, 1973) investigated the effects of air pollution on various dyed textiles by
11      conducting  field and controlled-environment laboratory studies.  For the field study, a wide
12      range of dyed fabric was exposed in light-tight cabinets at the same four urban and four rural
13      sites used in the Ajax studies. The study was carried out over a 2-year period, in eight
14      consecutive 3-mo seasonal  exposure periods. Color change data and air pollution and
15      weather measurements were analyzed to identify the factors that caused fading.  About two-
16      thirds of the fabrics studied showed appreciable fading.  Most of these fabrics faded
17      significantly more at urban sites than at rural sites.  The small amount of fading evidenced
18      by the samples exposed at extreme temperatures and/or humidity indicated that these factors
19      by themselves have no effect on fading.  The samples also showed some seasonal variations
20      in fading.  In areas of high oxidant concentration, maximum fading occurred primarily in
21      summer and fall.  Fabrics exposed in Chicago, where SO2 concentrations are higher in the
22      winter, showed greater fading during this season.
23          The results of the outdoor fading study were used in a multiple regression analysis.
24      The analysis focused on 25 fabric dye samples, 23 of which showed SO2 to be a significant
25      variable.  Ozone was  also a significant contributor to fading of eight dyed fabrics and NO2 to
26      fading of seven dyed fabrics. The dominance of SO2 as a factor in fading may have been
27      complicated by soiling.
28          Beloin's laboratory study was designed to assess the effects of air pollutants,
29      temperature, and RH on the colorfastness of 30 samples selected from those exposed during
30      the field study.  Fabric samples were exposed to two concentrations of O3:  0.05 ppm and
31      0.50 ppm.   The laboratory  studies demonstrated that high O3 levels produced more

        December 1993                           5.329      DRAFT-DO NOT QUOTE OR CITE

-------
 1     significant fading in more fabric samples than did low levels. Visible fading did occur hi
 2     about one-third of the sensitive fabrics (cellulose acetate, viscose, and cotton muslin with red
 3     and blue dyes) exposed to O3 concentrations of 0.05 ppm.  These levels are similar to those
 4     frequently found in metropolitan areas.  The laboratory study also demonstrated that high RH
 5     (90%) is a significant factor in promoting and accelerating O3-induced fading.
 6          Haynie et al.  (1976) and Upham et al. (1976)  reported on the degree of fading of three
 7     different drapery fabrics exposed in a laboratory chamber to combinations of high and low
 8     O3 concentration (0.5 and 0.1 ppm, respectively), high and low RH (90 and 50%,
 9     respectively), and high and  low concentrations of NO2 and  SO2.  The three commercially
10     obtained fabrics selected for this study were a royal blue rayon-acetate, a red rayon-acetate,
11     and a plum cotton duck. The samples were exposed in the chamber for periods of 250, 500,
12     and 1,000 h; the degree of  fading was measured with  a color difference meter.  The fading
13     of the plum-colored material was statistically related to RH and the NO2 concentration.  For
14     the red and blue fabrics, only RH appeared to be a  significant factor.  The effects of
15     concentrations of O3 on the amount of fading of these dyes were not statistically significant,
16     even after exposure for 1,000 h to 0.5 ppm, levels much higher than typical ambient
17     exposures.
18          Haylock  and Rush (1976, 1978) studied the fading of anthraquinone dyes on nylon
19     fibers.  In the  first test, nylon carpet  yarn dyed with Olive  I (0.081 % Celliton Pink RF,
20     0.465% Celliton Yellow GR, 0.069% Celliton Blue FFRN) and Olive H (0.082% Latyl
21     Cerise Y, 0.444%  Celliton  Yellow GA, 0.143% Cellanthrene Blue CR) was exposed  to
22     varying levels of temperature, RH, and O3.  Material dyed with Olive I and exposed  at 70%
23     RH, 40 °C (104 °F), and 0.2 ppm of O3 showed visible fading after 16 h of exposure.
24     At 90% RH, similar fading occurred  in less than 4  h.  Under the same RH and temperature
25     conditions, increasing the O3 concentration from 0.2 to 0.9 ppm resulted in a parallel
26     increase in fading.  Samples in knitted sleeve form  demonstrated much greater susceptibility
27     to O3 attack than samples in skein form.
28           Using Disperse Blue 3 and Disperse Blue 7 dyes exposed to constant conditions of
29     40 °C (104 °F), 90%  RH, and 0.2 ppm of O3, Haylock and Rush  (1976) investigated  the
30     effect on fading of changing the fiber cross section, the fiber draw ratio, and the method of
31     setting the nylon fibers with steam heat.  They found  that increasing the surface area  of the

       December 1993                          5-330      DRAFT-DO NOT QUOTE OR CITE

-------
 1      fibers resulted in an increased fading rate. Increasing the fiber draw ratio reduced dye
 2      fading, and increasing the heat-setting temperature decreased resistance to fading in disperse
 3      dyes.
 4          The effect of high temperature and high humidity for induction of O3 fading in nylon
 5      was further confirmed by the additional work of Haylock and Rush (1978). Their studies
 6      showed a good correlation between accelerated O3 fading in the laboratory and in outdoor,
 7      in-service exposure, during which temperature and humidity extremes were common.
 8      Control samples exposed indoors, however, where temperatures and humidities were lower,
 9      did not exhibit nearly the same magnitude of fading as the laboratory samples.
10          Huevel et al. (1978) investigated the importance of the physical nature of Nylon 6 yarns
11      on the O3 fading behavior of a disperse blue dye.  Samples of Nylon 6 yams  dyed avocado
12      green with a dye mixture including Disperse Blue 3 were exposed in a laboratory cabinet to
13      0.5 ppm of O3 at 40 °C and an RH of 85%.  Huevel et al. found that the microfibril
14      diameter and specific surface area of the fiber were the fiber characteristics most closely
15      related to O3 fading, thus confirming suspicions expressed earlier by Salvin (1969).
16          Nipe (1981) summarized the results of a 3-year study to establish the relationship
17      between in-service fading of carpets in a home versus O3 fading as determined by the
18      American Association of Textile Chemists and Colorists (AATCC) Standard Test Method
19      129, Colorfastness to Ozone in the Atmosphere Under High Humidities.  (Measurements
20      were also taken to compare the  fading caused by oxides of nitrogen.)  The test carpets were
21      made of Nylon 6 and 66 dyed with two disperse and two acid  dye formulas.   Test samples
22      from the homes of 28 participants were returned every 3 mo for the 3-year period. The
23      exposure sites selected  for this long-term  study represented variations in home heating and
24      cooling, utilities, climate, and geographical locations. The carpet samples were placed in
25      areas as close as possible to the kitchen but away from exposure to  sunlight or any traffic.
26      No measurements of O3 concentrations were collected; however, an ozone sensitive sample
27      strip was included with each carpet sample.  Analysis of the sample strip enabled the
28      researchers to determine the relative ozone exposure of each carpet  sample.
29          Geographical location appeared to have a significant effect on fading. Test samples
30      from sites in the southeast and northeast  showed far more O3 fading than those in the west
31      and far west.  Test samples in homes with air conditioning exhibited less fading during the

        December 1993                         5.331      DRAFT-DO NOT QUOTE OR CITE

-------
 1     summer than those without air conditioning.  In all samples, much greater fading was caused
 2     by O3 during July, August, and September than in January, February, and March.
 3     Typically, O3 levels indoors are higher during the summer, when doors and windows are
 4     more likely to be open, thus allowing a greater exchange between inside and outside air.
 5     The results of the study of in-service interior carpet exposures were compared with the
 6     results of AATCC Test 129.  In a sample that performs satisfactorily through 1.08 cycles of
 7     O3  exposure in AATCC Test 129, there is a 98% probability against in-service fading over a
 8     1-year period.  A sample that performs satisfactorily through only 0.6 cycles of O3 testing
 9     has only a 90% probability of satisfactory performance after 1 year of in-service exposure.
10           Kamath et al. (1983) studied the effect of atmospheric O3 dye fading on nylon fibers.
11     Prior studies  had postulated that O3  does not penetrate into the fiber to destroy the dye, but
12     instead attacks the dye at the surface of the fiber.  Dye then diffuses outward from the fiber
13     interior because of the concentration gradient set up as the surface dye is destroyed.  Using
14     microspectrophotometry to test this postulated mechanism, Kamath et al. studied the diffusion
15     and destruction of C.I. Disperse Blue Dye 3 on Nylon 6 continuous filament yarn measuring
16     about 45 /*m in diameter.  With this method, they were able to generate a dye distribution
17     profile across the cross section of the fiber and to determine the diffusion coefficient of a dye
18     in the fiber.  The fibers were exposed in a controlled environment to O3 concentrations of
19     0.2 ppm for 2 to  120 h at a temperature of 40  °C and RH levels of 90%, 85%, and  65%.
20     The results of these laboratory studies indicated that RH has a significant positive effect on
21     fading, that destruction of the  dye begins near the surface of the fiber in the early stages of
22     exposure, and that O3 penetration into the fiber may be an important mechanism in
23     O3 fading. The dependence of fading rates on humidity was substantial. Even slight rises in
24     humidity from 85 to 90%  caused a significant increase in the extent of fading.  At 65% RH,
25     the fading rate drops dramatically.  This effect was attributed to the breakage of hydrogen
26     bonds in the  presence of water, which leads to a more open structure  with high segmented
27     mobility; this condition is more favorable to diffusion of O3 and disperse dyes.
28           A follow-on study by Moore et al. (1984) used the Kamath et al. (1983) approach with
29     a variety of dyes, yarns and treatments. Moore and coworkers used untreated, phenol treated
30     and steam treated Nylon 6 and Nylon 66 continuous filament yarns, with six disperse blue
31     and acid blue dyes.  Molecular weights of the dyes ranged from MW = 296 (Disperse Blue

       December 1993                          5-332      DRAFT-DO NOT QUOTE OR CITE

-------
 1     No. 3) to MW = 872 (Acid Blue No. 127). Dyed filaments were exposed to 0.2 ppm O3 at
 2     40  °C and 90% relative humidity for various periods up to 96 h. For Nylon 6, steam treated
 3     fibers faded more quickly than untreated fibers, while phenol treated fibers faded less
 4     quickly.  In Nylon 66, both treatments increased the rate of dye loss.  The authors attributed
 5     this effect, at least in part, to the change in morphology of the treated fibers.  Faster fading
 6     was attributed to higher diffusion rates of the dye in the fiber.  They also observed that low
 7     molecular weight dyes faded faster than high molecular weight dyes, again suggesting the
 8     dye mobility within the fiber (rate of diffusion of the dye molecules to the surface of fiber)
 9     played a significant role in the fading process. Cross-sectional analysis of the exposed fibers
10     showed that most of the dye loss appeared to occur due to reactions at the fiber surface and
11     that penetration of O3 into the fiber did not seem to be significant.
12           Salvin (1969)  reported that O3 and (to a lesser extent) NO2 caused dye fading of cotton
13     polyester/permanent press fabrics.  As summarized by Dorset (1972), O3  was found to be the
14     major fading agent, with nitrogen oxides also capable of causing fading, though to a lesser
15     extent.  Remedial measures to avoid this problem include selecting  dyes more resistant to
16     reaction with O3 and NO2, avoiding the use of magnesium chloride catalyst in the permanent
17     press process, and using different surfactants and softeners. The use of magnesium chloride
18     as a catalyst makes O3-sensitive  dyes more sensitive to  O3 (Dorset, 1972).  When the catalyst
19     is zinc nitrate,  dyes are more washfast and resistant to O3  fading.   The present use of a zinc
20     nitrate catalyst appears to have generally eliminated the problem of the prefading of dyes in
21     permanent press fabrics from O3 exposure.
22          Much of the research reported on dye fading is qualitative in  nature. Earlier studies
23     relied on comparisons among various geographical  locations and seasonal variations with
24     little attention given to actual concentration and exposure characterizations.  For several of
25     the initial field investigations  reported here,  neither O3  nor oxidant concentrations were
26     given; rather,  notations such as high versus low or urban versus rural were  the only
27     description of oxidant levels.  The few laboratory studies employed only two concentrations
28     of O3 at most,  making it nearly impossible to derive meaningful exposure-response
29     relationships.  Comparisons among studies are difficult owing to the various dye and fabric
30     combinations tested. Also, the importance of relative humidity on  O3  fading rate confounds
31     comparisons among many of the studies that did not use the same RH percentages.  Despite

       December 1993                          5.333      DRAFT-DO NOT QUOTE OR CITE

-------
 1     these shortcomings, the existing body of research clearly demonstrates a strong relationship
 2     between dye fading and O3 exposure.  A definitive study to develop exposure-response
 3     functions that covers a broad spectrum of fabric/dye combinations, O3 exposures, humidities
 4     and temperatures has not been  undertaken, although the available literature establishes the
 5     likely significant variables for  such a study.
 6
 7     5.10.3.3 Fiber Damage
 8          Sunlight, heat, alternate wetting and drying, and microorganisms are causative factors
 9     in the weathering and deterioration of fabrics exposed outdoors.  The  influence of O3 at
10     normal  ambient levels is generally small by comparison. Table 5-39 summarizes the
11     experiments of the effects of ozone on textile fibers.
12          Bogaty et al. (1952), as part of a program aimed at segregating some of the elements
13     that cause weathering,  carried  out experiments  to study the possible role of O3 in the
14     deterioration of cotton  textiles.  These investigators exposed samples of duck and print cloth
15     to air containing 0.02 and 0.06 ppm of O3. Samples were exposed both dry and wet and
16     tested for 50 days.  The wet samples were water-saturated once per week, and moisture was
17     added regularly so that the moisture content of the cloth was  never less than 50%. Similar
18     fabric samples were exposed to similar O3 concentrations with no moisture added, and
19     another control group was similarly wetted but exposed to clean (O3-free) air.  After
20     exposure to O3, the wetted samples showed a loss in breaking strength of approximately
21     20%.  The wet print control cloth showed a loss in breaking  strength  of only half this
22     amount. The study showed that low levels of O3 degrade cotton fabrics if they are
23     sufficiently moist.  Bogaty et al. surmised that  an estimated 500 to 600 days of natural
24     exposure might be required to  reach a stage of degradation similar to that caused by a 50-day
25     exposure to O3 alone.  Because unprotected fabrics typically  reach a much more advanced
26     state of decay after such long exposures to weathering, Bogaty et al. concluded that the effect
27     of O3 is slighter than that of other agents.   Although not noted by Bogaty et al., the O3 and
28     increased moisture  may have caused the formation of hydrogen peroxide (H2O2), which
29     could account for the loss in breaking strength.
30           Morris (1966) also studied the effects of  O3 on cotton.  Samples were exposed in the
31     absence of light to  0.5 ppm of O3  (more than four times the  National Ambient Air Quality

       December 1993                          5-334      DRAFT-DO  NOT QUOTE OR CITE

-------
d
n>
O-    Fiber
i-l
                     TABLE 5-39.    LABORATORY AND FIELD STUDDZS OF THE EFFECTS OF OZONE ON FIBERS
                             Concentration
                                (ppm)
                   Exposure
                       Environmental
                         Variables
                                                                                                               Effects
                                                                                                                                                    References
       Cotton


       Cotton

       Cotton
       Modacrylic,
       Acrylic,
       Nylon 66,
       Polyester

       Nylon
0.02 and 0.06     50 days
    0-5

    1 -0


    °--
    0-03
50 days

60 days


7 days
              Cloth, both wet and dry
                                                          21 °C, 72% RH
O3 exposed wetted samples had 20% loss of breaking
strength.

No loss of breaking strength.
                                                           25 °C, periodic washing or wetting Washed O3 exposed fabrics had 18% loss of breaking
                                                                                         strength .
Bogaty et al. (1952)


Morris (1966)

Kerr et al. (1969)
                              48 °C, 39% RH
                              Artificial sunlight, wetting
                                                                                        No effect on modacrylic and polyester. Slightly reduced     Zeronian et al. (1971)
                                                                                        breaking strength in acrylic and nylon.
                Up to 445 days  Exposed in industrial warehouse    Loss of dyeability
                                                                                                                                           Makansi (1986)
U)
 d
 o
 25
I
8

-------
 1     Standard [NAAQS] of 0.12 ppm) for 50 days in a chamber maintained at 70 °F (21 °C) and
 2     72% RH. No appreciable effect on breaking strength was found.  Apparently, the moisture
 3     content of the cotton was not high enough to produce the degradation that Bogaty et al.
 4     (1952) measured in wet cotton samples, even though the concentration of O3 was
 5     considerably higher.
 6          The laboratory study of Kerr et al. (1969) examined the effects of the periodic washing
 7     of dyed cotton fabrics exposed to O3 and the amount of fading and degradation of moist,
 8     dyed fabrics exposed  to O3.  They exposed samples of print cloth, dyed with CI Vat Blue 29,
 9     in a chamber to a continuous supply of purified air containing O3 concentration levels of
10     1 ± 0.1 ppm. The sampks were exposed at room temperature (25 °C) in the absence of
11     light,  and a shallow container of water was kept on the chamber floor to increase the
12     humidity. Samples were  withdrawn from the chamber after 12, 24, 36, 48, and 60 days.
13     After an exposure period  of 60 days, which included either 20 washing or 20 soaking
14     treatments, the change in strength of control fabrics was not significant.  By comparison, the
15     fabrics exposed to O3 changed significantly; the loss in strength of the washed fabrics  was
16     18%, and that of the soaked fabrics, 9%.  Fading was also evident in the fabrics exposed to
17     O3, but not in the control samples.  Differences in the amount of fading between the washed
18     and soaked samples were evident, but the reason for the differences was not. Kerr et al.
19     concluded that washing in hot,  soapy water may have affected the properties of the dye.
20          In laboratory studies,  Zeronian et al. (1971) simultaneously exposed modacrylic
21     (dynel), acrylic (orlon), Nylon  66, and polyester (dacron) fabrics to artificial sunlight  (xenon
22     arc) and charcoal-filtered air contaminated with 0.2 ppm of O3 at 48 °C (118 °F) and 39%
23     RH.  During exposure, the fabric samples were sprayed with water for 18 min every 2 h.
24     Ozone damage was measured by comparing these samples with fabrics exposed to the same
25     environmental conditions without O3.  After exposure for 7 days,  Zeronian et al.  found that
26     O3 did not affect the modacrylic and polyester fibers.  The exposure did seem to affect the
27     acrylic and nylon fibers  slightly by reducing breaking strength. The degree of difference,
28     however, in the change of fabric properties between those exposed to light and air and those
29     exposed to light and air containing 0.2 ppm of O3  was not significant.
30           Ageing of nylon yarns causes a reduction  in the dyeability of the yarn.  Ageing is
31     caused by the reaction of amine end groups in the filament skin with O3 as well  as other

       December 1993                          5-336      DRAFT-DO NOT QUOTE OR CITE

-------
  1      pollutants (NOX, SO2, etc.). This phenomenon is well known within the textile trade and
  2      procedures  such as minimizing time from yarn production to yarn dyeing are in place to
  3      reduce problems of ageing.  Makansi (1986) investigated the relationship between yam
  4      ageing as defined by reduction in dyeability and pollutant levels in yarn storage warehouses.
  5      Makansi assessed the yam dyeability with Acid Blue 45  and Acid Blue 122 dyes of exposed
  6      test fiber versus unexposed control samples.  Gaseous pollutant concentrations in the
  7      warehouse were either estimated using nearby air quality station data or measured twice
                                                                      Tl^f
  8      weekly during the tests using commercial sampling tubes (Draeger   Tubes).  Yarn samples
  9      were exposed for up to one-year of ageing. Makansi found that dyeability decreased
 10      proportionally with the O3 exposure during storage. Dyeability as weight of dye absorbed
 11      for Acid Blue 45 decreased over 75 % for Nylon 66 stored in the warehouse at an average
 12      concentration of .03 ppm O3. It was not possible to statistically isolate the effects of
 13      O3 exposure from other pollutant exposures for the samples for these tests; thus other factors
 14      besides O3  may have contributed to the loss in dyeability.  Makansi  suggested that yarns
 15      should be dyed as quickly as possible after manufacture or should be stored in airtight
 16      wrappings to prevent ageing.
 17           In general, the contribution of O3  to degradation of fabrics has not been quantified
 18      well.  Bogaty et al. (1952) concluded that the effects of other factors (sunlight, heat, wetting
 19      and drying, and microorganisms) far  outweighed the effects of O3 on cotton duck and print
 20      cloth.  The  work by Morris (1966) and Kerr et al.  (1969) does point to the synergistic effect
 21      of moisture and O3 as an important ingredient in material degradation, possibly caused by the
 22      formation of a more potent oxidizing agent.  Finally, the work of Zeronian et al.  (1971) also
 23      indicates little if any effect of O3 on synthetic fibers.  Thus, it appears that O3 has little if
 24      any effect on textiles, fibers, and synthetic cloth exposed outdoors.  Because most fabrics  are
 25      used primarily indoors where they are partially shielded from O3 exposure, O3  damage to
 26      textile fibers is considered an insignificant problem. This was a finding of Murray et al.
 27      (1985) in a  study of material damage and costs in the Los Angeles area, an area with
28      relatively high ambient ozone concentrations.
29
30
       December 1993                          5.337      DRAFT-DO NOT QUOTE OR CITE

-------
 1     5.10.3.4  Paint Damage
 2           A paint surface may suffer several types of damage that affect its usefulness,  including
 3     cracking, peeling, erosion, and discoloration.  Of these, erosion (i.e., wearing away of the
 4     paint surface) is the type of damage most often studied with respect to the impact of gaseous
 5     pollutants on architectural and coil coating finishes.  (Coil coatings are industrial,
 6     continuous-dip process finishes typically applied to sheet metal).  Studies of paint cracking
 7     and peeling have focused on the effects of moisture and have  not dealt with the possible
 8     influence of ambient pollutants on these types of finishes.
 9           Several damage functions for O3-induced erosion of paint have been reported in the
10     literature.  Such reports  are based on either accelerated chamber studies or long-term outdoor
11     exposure studies.  Unfortunately, all studies to date have shortcomings that render  their
12     results questionable in regards to actual exposures. Damage to a paint surface is the
13     cumulative effect of the  conditions to which the surface is exposed, including various
14     combinations of temperature, moisture, sunlight, and pollution level.  No exposure study to
15     date has been able  to match all factors exactly to separate the impact of O3 from the other
16     factors.  Table 5-40 summarizes the studies of the effect of O3 on architectural and industrial
17     paint and coating systems.
18           In a laboratory chamber exposure study, Haynie et al. (1976) exposed oil-based house
19     paint, latex house paint, vinyl coil coating, and acrylic coil coating to 0.5 and 0.05 ppm
20     concentrations of SO2, NO2,  and O3 in various combinations. Statistically significant effects
21     of O3-caused damage were observed on the vinyl coil coating and the acrylic coil coating.
22     There was a positive interaction between O3 and RH on the vinyl coil coating and  a positive
23     direct O3 effect on the erosion rate of the acrylic coil coating. The rate of erosion was low,
24     however, and both vinyl and acrylic coil coatings were shown to be very durable.  A linear
25     regression for the acrylic coil coating data gives:
26
27                                Erosion rate = 0.159 +  0.000714 O3                      (5-1)
28
29      where erosion rate  is in /xm/year and O3 is /xg/m .
30           Although the O3 effect on this coating was found to be  statistically significant, it has no
31      practical significance because the erosion rate is so slow; at 0.12 ppm of O3, the erosion rate

        December 1993                           5-338      DRAFT-DO NOT QUOTE OR CITE

-------
                      TABLE 5-40.  LABORATORY AND FIELD STUDIES OF THE EFFECTS OF OZONE ON
I
cr
ft
1— '


Paint/Coating Type
Latex house paint
Oil house paint
Vinyl coil coating
Acrylic coil coating
Automotive refmish
Latex

Substrate
Aluminum
panels
Stainless
steel panels
AK^ttllHA.1
Concentration
(ppm) Exposure
0.05 and 0.5 to l,000h
0.1 and 1.0 to 1,000 h
UKJVLi/lTMJJUO 1K.LA1
Environmental
Variables
Chamber exposures with SOj,
N02, 03, 50 and 90% RH
13 and 35 °C, artificial dew
and sunlight cycles.
Chamber study with SO2,
70 to 100% RH, 50 to 65 °C,
^ fAJIMO AMU \s\JAL.
Effects
Very slow erosion of coil
coatings
Although 1 ppm O3 produced
significant changes in
LNtja
Comments Reference
Haynie et al. (1976)
Cambell et al. (1974)
u>
     Coil coating
     Industrial maintenance
     coating
     Oil house paint
artificial dew and sunlight
cycles.
finishes, 0 1 ppm O3 did not
produce statistically increased
erosion
                                 4 sites, rural to to 24 mo
                                   industrial
                                                       Field study.
                                             No environmental
                                             measurements conducted.
                                                                              Erosion greater in urban
                                                                              areas.
Latex house paint
Oil house paint
Stainless 0.006 to 0.055 3 to 30 mo Field study.
steel
Effects of O3 not
independently statistically
significant.
Nine sites around St. Louis Mansfeld (1980)

-------
 1     is 0.33 /urn/year.  At an average annual O3 level of 0.05 ppm, this regression predicts that a
 2     20-jum-thick coating would last over 80 years.
 3          In a comprehensive study by Campbell et al.  (1974), panels painted with different
 4     exterior paints (automotive refinish, latex coating, coil coating, industrial maintenance
 5     coating, and oil-based house paint) were exposed to air pollutants in an environmental
 6     chamber under accelerated weathering conditions.  The panels were exposed to low
 7     (0.1 ppm) and high (1.0 ppm) concentrations of O3 and SO2.  After exposure, the panels
 8     were examined by measuring erosion, gloss, surface roughness, tensile strength, attenuated
 9     total reflectance (ATR), and the surface effects revealed by scanning electron microscopy and
10     infrared examination.  The panels were examined after 0, 400, 700, and 1,000 h of chamber
11     exposure (considered as equivalent to 0, 200, 350,  and 500 days, respectively, of exposure).
12          In general, exposures to 1 ppm of O3 produced greater increases hi erosion rates than
13     did clean air.  Concentrations of this magnitude, however, do not  represent typical ambient
14     exposure levels of O3. At the more representative  level of 0.1 ppm, O3 did not produce
15     statistically significant increases in erosion rates. The various finishes produced a variety of
16     changes for the other measures. Some finishes  lost gloss or showed changes in ATR, but
17     O3 exposure did not produce consistent changes over the suite of finishes examined.
18          In conjunction with Campbell's chamber studies, field measurements  were made of the
19     erosion of paint from test panels exposed to outdoor environments consisting of a clean, rural
20     atmosphere (Leeds, North Dakota); a moderately polluted atmosphere  (Valparaiso, Indiana);
21     a heavily polluted (SO2) atmosphere (Chicago, Illinois); and a high-oxidant, moderately
22     polluted atmosphere (Los  Angeles,  California).  The  results of this study showed that paint
23     erosion was much greater in the polluted areas than in relatively clean, rural areas.  The
24     highest erosion rates were observed for the coil coating and oil-based house paints at the
25     Chicago and Los Angeles exposure sites.  Since meteorology and  air quality were not
26     measured at the exposure sites, correlation of film  damage with the environmental parameters
27     was not possible.  The study does suggest that SO2 exerts an  adverse effect on exterior paints
28     with calcium carbonate as an extender pigment.  The coil coating and oil house paints were
29     formulated with calcium carbonate. Oxidants were probably  reacting with the organic binder
30     of the coil coating and oil  house paints, although no  mechanism for this reaction was
31     developed from this exposure study.

       December 1993                           5-340       DRAFT-DO NOT QUOTE OR CITE

-------
  1           In an outdoor exposure test of the effects of air pollutants on materials, Mansfeld
  2      (1980) exposed latex and oil-based house paints as well as galvanized steel, weathering steel,
  3      stressed aluminum, silver,  marble, and nylon at nine test sites in St. Louis, Missouri.
  4      In conjunction with the material exposures, measurements of meteorological parameters, O3,
  5      oxides of nitrogen, total hydrocarbons, total sulfur, SO^, and hydrogen sulfide were made.
  6           Haynie and Spence (1984) analyzed Mansfeld's (1980) St. Louis data accounting for
  7      covariances among the pollutant and meteorological variables.  They analyzed the paint
  8      damage data and found significant correlations of O3 flux with time, temperature, and NO2
  9      flux for the experimental period. While Haynie and Spence expected O3 to attack the binder
 10      in latex paint, multiple regression analysis showed  little dependence of paint erosion on
 11      O3 flux.  They speculate that the effects of O3 are  masked by the covariance of O3 with
 12      temperature and oxides of nitrogen.
 13
 14      5.10.3.5  Cultural Properties Damage
 15           Ozone-induced degradation of cultural properties (e.g., fine arts paintings) contributes
 16      to the deterioration and ultimately the loss of these unique objects.  Many cultural properties
 17      are expected to last indefinitely, and irreversible damage, even at a slow rate, is considered
 18      unacceptable by curators and the art community.
 19           A significant series of tests of the effects of O3 on a variety of artist's pigments and
 20      dyes  was  reported by Shaver et al. (1983); Grosjean et al. (1987); Whitmore et al. (1987);
 21      Grosjean et al. (1988a,b); Whitmore and Cass (1988); Grosjean et al. (1989); Cass et al.
 22      (1991) and Grosjean et al. (1993). The experiments are  summarized in Table 5-41.  The
 23      doses of O3 applied during these tests were the equivalent of less than 10 years exposure in a
 24      typical air conditioned indoor environment. Many  pigments, and notably traditional organic
 25      pigments such as indigo, were found to be very sensitive to O3 exposure.  Many of the
 26      affected pigments underwent significant color changes  upon exposure to O3, and some were
 27      virtually completely consumed producing colorless  reaction products.  Cass et al. (1991)
28      noted that O3 damage to artwork is proportional to  the O3 exposure (concentration  x time).
29      Because artworks are intended to have long service lives and their appearance is important,
30      fading is generally considered to be  unacceptable, and  even low concentrations for  long
       December 1993                           5.34!       DRAFT-DO NOT QUOTE OR CITE

-------
TABLE 5-41. LABORATORY STUDIES OF THE EFFECTS OF
                     :>
n»
1
•o
u>










<-n
i
N)


d
£
^
H
O
O


*Q
Q
H
o
§
o
L/^Ui^JC,
Pigment Types Substrate Concentration
Seventeen Artists' Paper 0.4 ppm
watercolor
pigments



Alizarin, Silica Gel 0.4 ppm
Alizarin crimson, Cellulose 0.4 ppm
anthraquinone — —
Teflon 10 ppm

Sixteen traditional Paper 0.4 ppm
organic colorants


Indigo, Teflon 10 ppm
dibromoindigo,
thioindigo,
tetrachlorothioin-
digo




Curcumin Cellulose, 0.4 ppm
Watercolor 0.4 ppm
Paper, Silica Gel
— —
Teflon 10 ppm


, \JW f\K.LLOLO JTlAjlVJLn/m 1 a P.
ITMJ U I JCA3
Environmental
Exposure Variables Effects
95 days 23 °C
47% RH




95 days 22 °C
95 days 50% RH
— —
18-80 h 24 °C
<40% RH
12 weeks 23 °C
50% RH


4 days 24 °C
5% RH







95 days 25 °C
95 days 50% RH

— —
4 days 24 °C
^20% RH

Alizarin-based
watercolors were
very sensitive;
other pigments
showed lesser
degrees of fading.
Each pigment
tested faded on all
substrates.


Eleven colorants
were reactive with
O3, three were
possibly reactive.
All indigo,
dibromoindigo
consumed.
Thioindigo and
tetrachlorothioin-
digo were much
less reactive and
still retained much
color.
Faded rapidly on
all substrates
producing colorless
products.




Comments
Also
investigated
fading on
Japanese wood-
block print.

Presented
possible reaction
mechanisms and
products.



Reference
Shaver et al
(1983)




Grosjean et
(1987)



..





al.




Whitmore et al.



Presented
possible reaction
mechanisms.






Somewhat
slower fading
on watercolor
paper.



(1987)


Grosjean et
(1988a)







Grosjean et
(1988b)








al.








al.







-------
TABLE 5-41 (cont'd). LABORATORY STUDIES OF THE EFFECTS OF
         OZONE ON ARTISTS' PIGMENTS AND DYES
8"
^ Pigment Types Substrate Concentration Exposure
vo Traditional Paper, Silk Cloth 0.4 ppm 12 weeks
Japanese colorants
and dyes

Triphenylmethane Teflon 10 ppm 4 days
colorants




Alizarin Crimson Watercolor Paper 0.4 ppm 7 days

I
•£»
w Various artists' Watercolor Paper Mixture 12 weeks
colorants Cellulose 0.2 ppm O3
0.01 ppm PAN
O 0.08 ppm NO2
C
3

O

§ -
O
cl
O
o
Environmental
Variables Effects
22 °C Several organic
50% RH and one inorganic
pigment faded
significantly.
24 °C Found that while
<20% RH some are not
affected, those
colorants with
unsaturated C-C
bonds may fade.
22 °C Severe fading.
50% RH


16 to 26 °C 11 colorants-
46to83%RH negligible
changes
12 colorants-
small changes
3 colorants-
modest changes
9 colorants-
substantial
changes.





Comments Reference
Also investigated Whitmore and
fading one. 1810 Cass (1988)
Japanese
woodblock print.
Presented Grosjean et al.
possible reaction (1989)
mechanisms.



Framed sample Cass et al.
behind glass (1991)
exhibited virtually
no fading.
Grosjean et al.
(1993)













-------
 1     periods of time can lead to noticeable fading.  Grosjean et al. (1987) suggest that
 2     formulations of substitute pigments be developed with O3 sensitivity in mind.
 3          Druzik et al.  (1990) investigated the indoor/outdoor O3 concentration ratios at
 4     11 museums, art galleries, and historical houses in the Los Angeles, CA, area.  They found
 5     that the indoor/outdoor ratio of 8-h average O3 concentrations ranged from 0.10 to 0.87.
 6     The ratio was strongly dependent on the type of building ventilation. Buildings with high air
 7     exchange rates (ca. 2 to 3 air changes per hour) air ventilation had the highest indoor/outdoor
 8     ratios. Low exchange rate buildings (ca. less than one air change per hour) and buildings
 9     with air conditioning systems had significantly lower indoor/outdoor O3 concentration ratios.
10          De Santis et al. (1992) investigated concentrations of SO2, HNO3, HONO, and O3 as
11     well as paniculate  sulfate, nitrate and ammonium in the Galleria degli Uffizi in Florence for
12     a five day period.  Although the museum was equipped with an air conditioning system,
13     O3 concentrations in the galleries correlated strongly with  outdoor O3 concentrations.  Indoor
14     hourly average O3 concentrations ranged from 0.019 to 0.030 ppm. To reduce
15     concentrations in the galleries, they suggested that the Uffizi's air handling system be
16     upgraded to include filtration and modified to include less make-up air.  Cass et al. (1991)
17     and Grosjean et al. (1993) suggest that museums design and maintain air conditioning and air
18     filtration systems to control the concentrations of oxidants in order to protect their
19     collections.  Cass et al.  (1991) note that framing behind glass is an  effective means of
20     protecting oxidant sensitive pigments.  Grosjean and Parmar (1991) found that activated
21     carbon and Purafil (4%  potassium permanganate on neutral activated alumina) could be used
22     to reduce ozone and oxidant concentrations in museum display cases.
23
24     5.10.4  Economics
25     5.10.4.1  Introduction
26           Damage to materials from O3 is usually expressed in terms of one or both of the
27     following two general classes of costs to producers and consumers: (1) O3-accelerated
28     replacement and repair costs, as when the service life and/or aesthetics of a  material are
29     impaired, and (2)  increased avoidance costs, as when certain industries (e.g., tires, plastics,
30     paints, dyes, and fabrics) are obligated to incur expenditures for antiozonant research and
        December 1993                          5-344      DRAFT-DO NOT QUOTE OR CITE

-------
 1      development, substitute processes and materials, additives and formulations, product
 2      packaging, advertising, etc., in order to offset sales losses that would otherwise occur.
 3           In theory, the approach selected should depend on the observed behavior of the
 4      producers and consumers of the materials in question, and the type of damage to which they
 5      are reacting.  In practice, the existing empirical estimates of O3 damage to materials are far
 6      from reliable.
 7
 8      5.10.4.2  Methods of Cost Classification and Estimation
 9           Computation of accelerated replacement is probably the most widely applied method of
10      estimating the costs of materials damage to air pollutants. In this approach a materials
11      damage function is developed to show the increase in physical damage for an increase in the
12      dose of the pollutant.  Then a cost schedule is constructed to  show how maintenance or
13      replacement  schedules are influenced by  the pollutant level.  Hershaft et al. (1978) note,
14      however, that this method usually assumes existing inventories, and does not take into
15      account substitutions of materials with more (or less) resistance to pollution.  As a result,
16      this method tends to overestimate the cost of damage from pollutant increases and to
17      underestimate the net savings realized from pollutant reductions.
18           A second approach considers avoidance costs.  This refers to practices such as adopting
19      alternative production processes and materials.  Some industries add  antiozonants to their
20      products, or change the chemical formulation of their output.  All of these  measures mitigate
21      the impact of O3 on the service life or aesthetics of the products in question.  Moreover,
22      these measures also require research, development, and implementation expenditures.
23      As such, estimation of these costs is conceptually and empirically difficult, since the
24      opportunity to use different materials changes in response to the level of O3 concentration.
25           A number of factors complicate the use of both the replacement and the avoidance
26      methodologies. Data on key variables are generally missing or merely assumed.  Lessening
27      the reliability of the final cost estimates are deficiencies in knowledge of  (1) the physical
28      damage functions; (2) the quantities and types of materials exposed to O3 indoors, outdoors,
29      and in respective regions  of the country; (3) the actual expenditures incurred for increased
30      replacement, maintenance, and avoidance that can be directly attributed to O3; (4) the
31      threshold O3 damage levels that prompt mitigating action; and (5) the range of substitution

        December 1993                          5.345       DRAFT-DO NOT  QUOTE OR CITE

-------
 1      strategies that can be used to ameliorate degradation.  On this latter point, few attempts have
 2      been made to identify current technology practices and possibilities. The variety of rubber
 3      compounds, paint mixtures, and fabric dyes reflects the number of proprietary formulations,
 4      and each formulation presumably  has a different response to O3 exposure.
 5          An additional complication is that repair, replacement, and substitution are frequently
 6      dominated by factors unrelated to O3 concentrations. This can lead to spurious correlations
 7      if studies are accepted uncritically.  For example, tire replacement may be high in a given
 8      region of the country because of high  O3 levels associated with automotive exhaust.
 9      Alternatively, it may be high simply because the total miles of automotive use per year are
10      higher in that region than in the nation as a whole.
11
12      5.10.4.3  Aggregate Cost Estimates
13          The important caveats identified  in the preceding discussion qualify the empirical data
14      presented in this and following  sections.  Table 5-42 summarizes reports of highly
15      aggregated estimates of oxidant damage to all materials.  Unfortunately, there are no known
16      recognized studies that are  more recent than those reported in the table.  For purposes of
17      gross comparison only, the figures are expressed in  1984 currency equivalents alongside
18      1970 currency equivalents, the base data  for the reference studies.  They do not, however,
19      represent 1984 supply-demand relationships, production technologies, or O3 concentrations.
20      It must be emphasized that the costs cited in 1984 currency equivalents therefore cannot be
21      considered true 1984 costs.  Although the data in Table 5-42 is reported to four significant
22      figures, the real accuracy of this information is much less.
23          Salmon (1970) was among the first  to attempt  to estimate the annual cost of air
24      pollution damage to materials.  His computation included the dollar value of annual materials
25      production, a weighted average economic life of each material included in his study, a
26      weighted average factor for the percentage of the material exposed to air pollution, and a
27      factor for increased labor to treat damaged materials.  Cost was defined as the value of the
28      material multiplied by the difference between  the rate of material deterioration in a polluted
29      urban versus an unpolluted rural environment.  All data, except for annual production levels
30      of materials, were assumed.
        December 1993                          5-346      DRAFT-DO NOT QUOTE OR CITE

-------
         TABLE 5-42.  SUMMARY OF DAMAGE COSTS TO MATERIALS BY OXTOANTS
                                (in Millions of 1970 and 1984 Dollars)
Study
Barrett and Waddell
(1973)
Mueller and
Stickney (1970)
Salmon (1970)
Salvin (1970)
Waddell (1974)
Yocom and
Grappone (1976)
Freeman (1979)

Elastomers/Plastics
NDa
500.0
(l,500)b
295.2
(915)
ND
ND
ND
ND
Materials Costs
Fabric/Dye
(260)
ND
358.4
(1,111)
83.5
(259)
ND
ND
ND

All
(3,878)
ND
653.6
(2,026)
ND
900.0
(2,790)
572.0
(1,773)
505.0
(1,566)
       aND = No data. Investigator(s) did not develop estimates in this category.
       b!984 dollars are listed parenthetically below 1970 dollars and reflect inflation (consumer price index) rather
        than real increases in costs.
 1          If it is assumed that O3 affected all of the fibers, plastics, and rubber in the study by
 2     Salmon,  then annual damage costs attributed to O3 would have been $2,026 million (1984$).
 3     Salmon did not consider O3-related damage to paint, since the dominant paint-damaging
 4     mechanisms are soiling and gaseous sulfur dioxide.  His costs refer to maintenance and
 5     replacement only, and do not allow for materials protection, substitution, etc.
 6          In discussing other limitations of his study, Salmon cautioned that his estimates were of
 7     potential loss, not of actual observed loss.  Despite this and other qualifications that lessen
 8     the usefulness of the figures derived, the Salmon study has been cited extensively and used
 9     quantitatively in a number of the subsequent studies cited here.
10          For example, the materials estimate by Barrett and Waddell (1973) is based primarily
11     on the work of Salmon (1970). Barrett and Waddell supplemented this by drawing on
       December 1993
5-347
DRAFT-DO NOT QUOTE OR CITE

-------
 1     Mueller and Stickney (1970) for damage costs on elastomers, and on Salvin (1970) for
 2     damage costs related to dye fading.  Combining some of these numbers, Barrett and Waddell
 3     stated that materials damage costs attributable to  oxidants alone were $3,878 million (1984$).
 4          Freeman (1979) reviewed earlier studies that categorized the cost of damage to
 5     materials. Using the work of Waddell (1974) and Salvin (1970), Freeman calculated that the
 6     materials damage costs attributable to oxidants and oxides of nitrogen were $2,031  million
 7     (1984$). Of this total, roughly 46% was damage to textiles and dyes (from Salvin  1970),
 8     while the remaining 54% was damage to elastomers (from Mueller and Stickney, 1970).
 9     Freeman then assumed a 20% reduction in oxidant levels since 1970, and went on to
10     conclude that the monetary benefits of controlling oxidants, oxidant precursors, and oxides of
11     nitrogen were between $170 and $510 million (1984$).  Freeman computed the savings
12     attributable to oxidant controls alone as $128 to $383 million (1984$).
13          Waddell (1974) likewise depended primarily on existing studies to calculate the national
14     cost of air pollution in 1970.  Waddell used  Salmon (1970), Salvin (1970),  Mueller and
15     Stickney (1970), and Spence and Haynie (1972) to  derive an estimate of $6,820 million
16     (1984$) as the total gross annual damage for materials losses in  1970 resulting from air
17     pollution. The component attributable to O3 and oxidants alone was $2,790 million (1984$),
18     within a wide range of $1,550 to $4,030 million  (1984$).
19          Yocom and Grappone (1976), in work  for the Electric Power Research Institute,
20     estimated that the cost of air pollution damage to materials was about $6,820 million (1984$)
21     in 1970. Of this total, O3 was estimated to be responsible for $1,773 million (1984$), or
22     some 26% of the total.
23          Because of the reliance of the later studies on the questionable data and unverified
24     assumptions contained in the earlier ones, the results compared here are of extremely limited
25     usefulness for cost-benefit purposes.  Updated research, using current economic evaluation
26     approaches,  should be undertaken to determine the costs of O3-induced damage.
27
28     5.10.5  Summary and Conclusions
29          Over four decades  of research show that 03 damages certain materials.  The materials
30     most studied in O3 research are elastomers and textile fibers and dyes. The amount of
        December 1993                          5-348      DRAFT-DO NOT QUOTE OR CITE

-------
  1      damage to actual in-use materials and the economic consequences of that damage are poorly
  2      characterized.
  3            Natural rubber and synthetic polymers of butadiene, isoprene,  and styrene, used in
  4      products like automobile tires and protective outdoor electrical coverings, account for most
  5      of the elastomer production in the United States.  The action of 03 on these compounds is
  6      well known, and dose-response relationships have been established and corroborated by
  7      several studies.  These relationships, however,  must be correlated with adequate exposure
  8      information based on product use.  For these and other economically important materials,
  9      protective measures have been formulated to reduce the rate of oxidative damage.  When
 10      antioxidants  and other protective measures are incorporated in elastomer production, the
 11      dose-cracking rate is reduced considerably, although the extent of reduction differs widely
 12      according to the material and the type and amount of protective measures used.
 13           The effects of O3 on dyes have been known for nearly four decades.  In  1955, Salvin
 14      and Walker exposed certain red and blue anthraquinone dyes to a 0.1 ppm concentration of
 15      O3 and noted fading,  which until that time was thought to be caused  by NQ^.  Subsequent
 16      work confirmed the fading action of O3 and the importance of relative humidity in the
 17      absorption and reaction of O3 in vulnerable dyes.  Both the type of dye and the material in
 18      which it is incorporated are important factors in a fabric's resistance  to O3.  Researchers
 19      found no effects from  O3  on royal blue rayon-acetate, red rayon-acetate, or plum cotton.
 20      On the other hand, anthraquinone dyes on nylon fibers were sensitive to fading from O3.
 21      Field studies and laboratory work showed a positive association between O3 levels  and dye
 22      fading of nylon materials.  At present, the available research is insufficient to quantify the
 23      amount of damaged material attributable to O3 alone.
 24           The degradation of fibers from exposure to O3 is poorly characterized. In general,
 25      most synthetic fibers like modacrylic and polyester are relatively resistant, whereas cotton,
 26      nylon, and acrylic fibers have greater but  varying sensitivities to the  gas. Ozone reduces the
 27      breaking strength of these fibers, and the degree of reduction depends on the amount of
28      moisture present.  The limited research  in this area indicates that O3  in ambient air may have
29      a minimal effect on textile fibers, but additional research  is needed to verify this conclusion.
30          The effects of O3 on paint are small  in comparison with those of other factors.  Past
31      studies have shown that, of various architectural and commercial paints, only vinyl and

        December 1993                          5.349      DRAFT-DO  NOT QUOTE OR CITE

-------
 1     acrylic coil coatings are affected, and that this impact has a negligible effect on the useful
 2     life of the material coated.  Preliminary results of current studies have indicated a statistically
 3     significant effect of O3 and relative humidity on latex house paint, but the final results of
 4     those studies are needed before conclusions can be drawn.
 5          A number of artists' pigments and dyes have been found to be sensitive to O3 and other
 6     oxidants.  Many organic pigments in particular are subject to fading or other color changes
 7     when exposed to O3.  While most, but not all, modern fine arts paints are more O3 resistant,
 8     many older works  of art are at risk of permanent damage due to O3 induced fading.
 9     Museums and private  collectors should take steps to ensure that susceptible artwork is
10     protected from O3  exposure.
11          For a number of important reasons, the estimates of economic damage to materials are
12     problematic.  Most of the available studies are now outdated  in terms of the
13     O3 concentrations, technologies, and supply-demand relationships that prevailed when the
14     studies were conducted.  Additionally, little was (and is) known about the physical damage
15     functions, and cost estimates were simplified to the point of not properly recognizing many
16     of the scientific complexities of the impact of 63.  Assumptions about exposure to
17     O3 generally ignored the difference between outdoor and indoor concentrations. Also,
18     analysts have had difficulty separating O3 damage from other factors affecting materials
19     maintenance and replacement schedules.  For the most part, the studies  of economic cost
20     have not had the resources to marshal factual observations on how materials manufacturers
21     have altered their technologies, materials, and methods in response to O3.  Rather, the
22     analysts have been forced to rely on assumptions in  this  regard, most of which remain
23     unverified through the present time.
24          It is apparent that a great deal of work remains to be done in developing quantitative
25     estimates of materials damage from photochemical oxidant exposures.  This is not meant to
26     deprecate the years of research reported in this document, for much has been gained in
27     refining the initial methodologies used for assessing  damage.  To date, the current state of
28     knowledge can still be summarized by the following quote from Yocom et al. (1985):
29
30
        December 1993                          5-350      DRAFT-DO NOT QUOTE OR CITE

-------
 1                "We have learned that some costs may be difficult to quantify either
 2            because they are minimal or because they are overshadowed by other factors,
 3            such as wear or obsolescence.  We have learned that damage functions are
 4            complex and are influenced by the presence of other pollutants and by
 5            weather.  We have learned that more accurate estimates of materials in place
 6            may be obtained using selective sampling and extrapolation.  And we have
 7            learned that a mere cost-accounting of damage does not present a true estimate
 8            of economic cost if it does not account for the welfare effects induced by shifts
 9            in the supply-demand relationship."
10
11
       December 1993                          5.35!      DRAFT-DO NOT QUOTE OR CITE

-------
 1     REFERENCES
 2
 3     Abeles, F. B.; Morgan, P. W.; Saltveit, M. E., Jr. (1992) Ethylene in plant biology. 2nd ed. San Diego,
 4            CA: Academic Press; pp. 414.
 5
 6     Adamowicz, W. L. (1991) Valuation of environmental amenities. Can. J. Agric. Econ. 39: 609-618.
 7
 8     Adams, R. M. (1986) Agriculture, forestry, and related benefits of air pollution control: a review and some
 9            observations. Am. J. Agric. Econ. 68: 464-472.
10
11     Adams, R. M.; Crocker,  T. D. (1989) The agricultural economics of environmental change: some lessons from
12            air pollution. J. Environ. Manage. 28: 295-307.
13
14     Adams, M. B.; O'Neill, E.  G. (1991) Effects of ozone and acidic deposition on carbon allocation and
15            mycorrhizal colonization of Pinus taeda L. seedlings. For. Sci. 37: 5-16.
16
17     Adams, R. M.; Rowe, R. D.  (1990) The economic effects of stratospheric ozone depletion on U.S.  agriculture:
18            a preliminary  assessment. J. Environ. Manage. 30: 321-335.
19
20     Adams, R. M.; Hamilton, S.  A.; McCarl, B. A. (1986a) The benefit of pollution control: the case of ozone and
21            U.S. agriculture.  Am. J. Agric. Econ. 68: 886-893.
22
23     Adams, R. M.; Callaway, J. M.; McCarl, B. A. (1986b) Pollution, agriculture and social welfare: the case of
24            acid deposition. Can.  J. Agric. Econ. 34: 3-19.
25
26     Adams, M. B.; Kelly, J.  M.; Edwards, N. T. (1988a) Growth of Pinus  taeda L. seedlings varies with family and
27            ozone exposure level. Water Air Soil Pollut. 38:  137-150.
28
29     Adams, R. M.; Glyer, D. J.; McCarl, B. A. (1988b) The NCLAN economic assessment: approach, findings and
30            implications. In: Heck, W. W.; Taylor, O. C.; Tingey,  D. T., eds. Assessment of crop loss from air
31            pollutants: proceedings of an international conference;  October 1987; Raleigh, NC. New York, NY:
32            Elsevier Applied  Science; pp. 473-504.
33
34     Adams, R. M.; Glyer, J. D.; Johnson, S. L.; McCarl, B. A. (1989a) A reassessment of the economic effects of
35            ozone on U.S. agriculture. JAPCA 39: 960-968.
36
37     Adams, R. M.; Berglund, O.; Musser, W. N.; Johnson,  S. L.; Musser, L. M. (1989b) User fees and equity
38            issues in public hunting expenditures: the case of the ring-necked pheasant in Oregon. Land Econ.
39            65: 376-385.
40                                                                                   .,
41     Adams, M. B.; Edwards, N.  T.; Taylor, G. E., Jr.; Skaggs, B. L. (1990a) Whole-plant  C-photosynthate
42            allocation in Pinus taeda: seasonal patterns at ambient and elevated ozone levels. Can. J.  For. Res.
43            20: 152-158.
44
45     Adams, M. B.; Kelly, J.  M.; Taylor, G. E., Jr.; Edwards, N. T. (1990b) Growth of five families of Pinus taeda
46            L. during three years of ozone exposure. New Phytol. 116: 689-694.
47
48     Adams, R. M.; Klingeman, P. C.; Li, H. W. (1990c) A bioeconomic analysis of water allocations and fish
49            enhancements, John Day Basin, Oregon. Corvallis, OR: Oregon State University; USGS grant
50           no. 14-68-0001-G 1479.
51
52     Adams, R. M.; Rosenzweig,  C.; Peart, R.; Ritchie, J.  et al. (1990d) Global climate change and U.S. agriculture.
53            Nature 345: 219-224.
54

         December 1993                              5-352        DRAFT-DO  NOT QUOTE OR CITE

-------
  1      Adaros, G.; Weigel, H. J.; Jager, H.-J. (1991a) Die Wirkung von Ozon auf Wachstums- und Ertragsparameter
  2            zweier Sommerweizensorten (Triticum aestivum L.) [Impact of ozone on growth and yield parameters of
  3            two spring wheat cultivars (Triticum aestivum L.)]. Z. Pflanzenkr. Pflanzenschutz 98: 113-124.
  4
  5      Adaros, G.; Weigel, H. J.; Jager, H. J. (1991b) Single and interactive effects of low levels of 03,  SO2 and NO2
  6            on the growth and yield of spring rape. Environ. Pollut. 72: 269-286.
  7
  8      Adaros, G.; Weigel, H. J.; Jaeger, H. J. (1991c) Concurrent exposure to SO2 and/or NO2 alters growth and
  9            yield responses of wheat and barley to low concentrations of O3. New Phytol. 118: 581-591.
10
11      Adaros, G.; Weigel, H. J.; Jager, H. J. (1991d) Wachstum und Ertrag von Sommerraps und Sommergerste unter
12            chronischem Ozonstress [Growth and yield of spring rape and spring barley as affected by chronic ozone
13            stress]. Z. Pflanzenkr.  Pflanzenschutz 98: 513-525.
14
15      Adedipe, N. O.; Hofstra, G.; Ormrod, D. P. (1972) Effects of sulfur nutrition on phytotoxicity and growth
16            responses of bean plants to ozone. Can. J. Bot. 50:  1789-1793.
17
18      Adomait,  E. J.; Ensing, J.; Hofstra, G. (1987) A dose-response function for the impact of 63 on Ontario-grown
19            white bean and an estimate of economic loss. Can. J. Plant Sci. 67: 131-136.
20
21      Ainsworth, N.; Ashmore, M. R. (1992) Assessment of ozone effects on beech (Fagus sylvaticd) by injection of  a
22            protectant chemical.  For. Ecol. Manage. 51: 129-136.
23
24      Ajax, R. L.; Conlee, C. J.; Upham, J. B. (1967) The effects of air pollution on the fading of dyed fabrics. J. Air
25            Pollut. Control Assoc.  17: 220-224.
26
27      Allen, L.  H., Jr. (1990) Plant responses to rising carbon dioxide and potential interactions with air pollutants.
28            J. Environ. Qual.  19: 15-34.
29
30      Allen, M. (1991) The ecology of mycorrhizae. New York, NY: Cambridge University Press; pp. 184.
31
32      Allen, O.  B.; Marie, B. A.; Ormrod, D. P.  (1987) Relative efficiency of factorial designs for estimating
33            response surfaces with reference to gaseous pollutant mixtures. J. Environ. Qual. 16: 316-320.
34
35      Alscher, R. G.; Amthor, J. S.  (1988) The physiology of free-radical scavenging: maintenance and repair
36            processes.  In: Schulte-Hostede, S.; Darrall,  N. M.; Blank, L. W.; Wellburn, A. R., eds. Air pollution
37            and plant metabolism. London, United Kingdom: Elsevier Applied Science; pp. 94-115.
38
39      Alscher, R. G.; Amundson,  R.  G.; Gumming, J. R.; Fellows, S.; Fincher, J.; Rubin, G.;  van Leuken, P.;
40            Weinstein, L. H. (1989) Seasonal changes in the pigments, carbohydrates and growth of red  spruce as
41            affected by ozone. New Phytol. 113:  211-223.
42
43      Amiro, B. D.; Gillespie, T. J.  (1985) Leaf conductance response of Phaseolus vulgaris to ozone flux density.
44            Atmos. Environ. 19: 807-810.
45
46      Amiro, B. D.; Gillespie, T. J.;  Thurtell, G.  W. (1984) Injury response of Phaseolus vulgaris to ozone flux
47            density. Atmos. Environ. 18: 1207-1215.
48
49      Amthor, J. S. (1988) Growth and maintenance respiration in leaves of bean (Phaseolus vulgaris L.) exposed to
50            ozone in open-top chambers in the field.  New Phytol.  110: 319-325.
51
52      Amthor, J. S.; Gumming, J. R. (1988) Low  levels of ozone increase bean leaf maintenance respiration. Can.
53            J.  Bot. 66: 724-726.
54


         December 1993                               5.353       DRAFT-DO  NOT QUOTE OR CITE

-------
  1      Amundson, R. G.; Raba, R. M.; Schoettle, A. W.; Reich, P.  B. (1986) Response of soybean to low
  2             concentrations of ozone: II. effects on growth, biomass allocation, and flowering. J. Environ. Qual.
  3             15: 161-167.
  4
  5      Amundson, R. G.; Kohut, R. J.; Schoettle, A. W.; Raba, R. M.; Reich, P. B. (1987) Correlative reductions in
  6             whole-plant photosynthesis and yield of winter wheat caused by ozone. Phytopathology 77: 75-79.
  7
  8      Amundson, R. G.; Alscher, R. G.; Fellows, S.; Rubin, G.; Fincher, J.; Van Leuken, P.; Weinstein, L. H.
  9             (1991) Seasonal changes in the pigments, carbohydrates and growth of red spruce as affected by exposure
10             to ozone for two growing seasons. New Phytol. 118: 127-138.
11
12      Andersen, C. P.; Rygiewicz, P. T.  (1991) Stress interactions and mycorrhizal plant response:  understanding
13             carbon allocation  priorities. Environ. Pollut. 73: 217-244.
14
15      Andersen, C. P.; Rygiewicz, P. T.  (1993) Effect of ozone on translocation to roots of Pinus ponderosa. Can.
16             J. For. Res.: in preparation.
17
18      Andersen et al.  (1990).
19
20      Andersen, C. P.; Hogsett, W. E.; Wessling, R.; Plocher,  M. (1991) Ozone decreases spring root growth and
21             root carbohydrate content in ponderosa pine the year following exposure. Can. J. For. Res.
22             21: 1288-1291.
23
24      Andersen et al.  (1992).
25
26      Anderson,  E. (1990) The ethical limitations of the market. Econ. Philos. 6:  179-205.
27
28      Anderson, R. L.; Brown, H. D.; Chevone, B.  I.;  McCartney,  T. C. (1988) Occurence of air pollution symptoms
29             (needle  tip necrosis and chlorotic mottling) on eastern white pine in the southern Appalachian Mountains.
30             Plant Dis. 72: 130-132.
31
32      Anderson et al.  (1990)
33
34      Anderson, J.  V.; Chevone, B. I.; Hess, J. L. (1992) Seasonal  variation in the antioxidant system of eastern white
35             pine needles: evidence for thermal dependence. Plant Physiol. 98: 501-508.
36
37      Andries, J. C.;  Diem, H. E. (1974) A study of ozone attack on elastomer surfaces by attenuated total reflectance
38             spectroscopy. J. Polym. Sci. Polym. Lett. Ed.  12: 281-286.
39
40      Andries, J. C.;  Rhee, C.  K.; Smith, R. W.; Ross, D. B.; Diem, H. E. (1979) A surface study of ozone attack
41             and antiozonant protection of carbon black loaded natural rubber compounds. Rubber Chem. Technol.
42             52: 823-837.
43
44      Aphalo, P. J.; Jarvis, P. G. (1991) Do stomata respond to relative humidity? Plant Cell Environ. 14: 127-132.
45
46      Ashmore, M. R. (1984) Effects of ozone on vegetation hi the United Kingdom. In: Grennfelt, P., ed.
47             Proceedings of the international workshop on the evaluation of the effects of photochemical oxidants on
48             human health, agricultural crops, forestry, materials and visibility; February-March; Goteborg, Sweden.
49             Goteborg, Sweden: Swedish Environmental Research Institute; pp. 92-104; report no. IVL-EM 1570.
50
51      Ashmore, M. R. (1988) A comparison of indices that describe the relationship between exposure to ozone and
52             reduction in the yield of agricultural crops [comments on article by Lefohn et al. (1988a)]. Atmos.
53             Environ. 22: 2060-2061.
54


         December 1993                              5.354       DRAFT-DO NOT QUOTE OR CITE

-------
  1      Ashmore, M. R.; Bell, J. N. B.  (1991) The role of ozone in global change. Ann. Bot. 67: 39-48.
  2
  3      Ashmore, M. R.; Onal, M.  (1984) Modification by sulphur dioxide of the responses of Hordeum vulgare to
  4             ozone. Environ.  Pollut. Ser. A 36: 31-43.
  5
  6      Ashmore, M. R.; Bell, J. N. B.; Mimmack,  A. (1988) Crop growth along a gradient of ambient air pollution.
  7             Environ. Pollut.  53: 99-121.
  8
  9      Atkinson, C. J.; Wookey, P. A.; Mansfield, T. A. (1991)  Atmospheric pollution and the sensitivity of stomata on
 10             barley leaves to abscisic  acid and carbon dioxide. New Phytol. 117: 535-541.
 11
 12      Aycock, M. K., Jr. (1972) Combining ability estimates for weather fleck in Nicotiana tabacum L. Crop Sci.
 13             12: 672-674.
 14
 15      Baldocchi, D. D.; Hicks, B. B.;  Camara, P. (1987) A canopy stomatal resistance model for gaseous deposition to
 16             vegetated surfaces. Atmos. Environ.  21: 91-101.
 17
 18      Ball, J. T.; Woodrow, I. E.; Berry, J. A. (1987) A model  predicting stomatal conductance and its contribution to
 19             the control of photosynthesis under different environmental conditions. In: Biggins, J., ed. Progress in
 20             photosynthesis research,  v. IV: proceedings of the  Vllth international congress on photosynthesis; August
 21             1986; Providence, RI. Dordrecht, The Netherlands: Martinus Nijhoff Publishers; pp. 221-224.
 22
 23      Barnard, J. E.; Lucier, A. A.  (1990) Changes in forest health and productivity in the United States. In: Acidic
 24             deposition: state  of science and technology, V. III.  Washington, DC: National Acid Precipitation
 25             Assessment Program; report no. 16.
 26
 27      Barnes, J.  D.; Brown, K. A. (1990) The influence of ozone; acid mist on the amount; wettability of the surface
 28             waxes in Norway spruce [Picea abies (L.) Karst.].  New Phytol. 114: 531-535.
 29
 30      Barnes, J.  D.; Davison, A. W. (1988) The influence of ozone on the winter hardiness of Norway spruce [Picea
 31             abies (L.) Karst.]. New Phytol.  108:  159-166.
 32
 33      Barnes, J.  D.; Pfirrmann, T. (1992) The influence of CC>2  and 03 singly and in combination on gas exchange
 34             growth and nutrient status of radish Raphanus sativus L. New Phytol. 121: 403-412.
 35
 36      Barnes, J.  D.; Davison, A. W.; Booth, T. A. (1988a) Ozone accelerates  structural degradation of epicuticular
 37             wax on Norway spruce needles.  New Phytol.  110:  309-318.
 38
 39      Barnes, J.  D.; Reiling, K.; Davison, A.  W.; Renner,  C. J. (1988b) Interaction between ozone and winter stress.
 40             Environ. Pollut.  53: 235-254.
 41
 42      Barnes, J.  D.; Eamus,  D.; Brown, K. A. (1990a)  The influence of ozone, acid mist and soil nutrient status on
 43             Norway spruce [Picea abies (L.) Karst.]: I. plant-water relations. New Phytol. 114: 713-720.
 44
 45      Barnes, J.  D.; Eamus,  D.; Brown, K. A. (1990b)  The influence of ozone, acid mist and soil nutrient status on
 46             Norway spruce [Picea abies (L.) Karst.]: II. photosynthesis, dark respiration and soluble carbohydrates
 47             of trees during late autumn. New Phytol. 115: 149-156.
 48
 49      Barnes, J. D.; Velissariou, D.; Davison, A. W.; Holevas, C. D. (1990c) Comparative ozone sensitivity of old
 50             and modern Greek cultivars of spring wheat. New Phytol. 116: 707-714.
51
 52      Barrett, S.  C. H.; Bush,  E. J.  (1991) Population processes  in plants and the evolution of resistance to  gaseous air
53             pollutants. In: Taylor,  G. E., Jr.; Pitelka,  L. F.; Clegg, M. T., eds. Ecological genetics and air
54             pollution. New York, NY:  Springer-Verlag; pp. 137-165.


         December 1993                                5.355        DRAFT-DO NOT QUOTE  OR CITE

-------
  1      Barrett, L. B.; Waddeil, T. E. (1973) Cost of air pollution damage: a status report. Research Triangle Park, NC:
  2             U.S. Environmental Protection Agency, National Environmental Research Center; publication no. AP-85.
  3             Available from: NTIS, Springfield, VA; PB-222040.
  4
  5      Bazzaz, F. A. (1990) The response of natural ecosystems to the rising global CO2 levels Annu. Rev. Ecol. Syst.
  6             21:  167-196.
  7
  8      Beckerson, D.  W.; Hofstra, G.; Wukasch, R. (1979) The relative sensitivities of 33 bean cultivars to ozone and
  9             sulfur dioxide singly or in combination in controlled exposures and to oxidants in the field. Plant Dis.
10             Rep. 63: 478-482.
11
12      Bell, J. N. B.; Ashmore, M. R.; Wilson, G.  B. (1991) Ecological genetics and chemical modifications of the
13             atmosphere. In: Taylor, G. E., Jr.; Pitelka, L.  F.; Clegg, M. T., eds. Ecological genetics and air
14             pollution. New York, NY: Springer-Verlag;  pp. 33-59.
15
16      Beloin, N. J. (1972) Fading of dyed fabrics by air pollution. Text.  Chem. Color. 4: 77-82.
17
18      Beloin, N. J. (1973) Fading of dyed fabrics exposed to air pollutants. Text. Chem. Color. 5: 128-133.
19
20      Bender, J.; Weigel, H.-J.; Jager, H.-J. (1990) Regression analysis  to describe yield and metabolic responses of
21             beans (Phaseolus vulgaris) to chronic ozone  stress. Angew  Bot. 64: 329-343.
22
23      Bender, J.; Weigel, H. J.; Jager, H. J. (1991) Response of nitrogen metabolism in beans (Phaseolus vulgaris L.)
24             after exposure to ozone and nitrogen  dioxide, alone and in sequence. New Phytol. 119: 261-267.
25
26      Bennett, J. H. (1979) Foliar exchange of gases. In: Heck, W. W.;  Krupa, S. V.; Linzon, S. N., eds.
27             Methodology for the assessment  of air pollution effects on vegetation:  a handbook from a specialty
28             conference; April 1978; Minneapolis, MN. Pittsburgh, PA: Air Pollution Control Association;
29             pp.  10-1-10-29.
30
31      Bennett, J. P.; Runeckles, V. C. (1977)  Effects of low levels of ozone on plant competition. J. Appl. Ecol.
32             14: 877-880.
33
34      Bennett, J. H.; Hill, A. C.; Gates, D. M.  (1973) A model for gaseous pollutant sorption by leaves.  J. Air Pollut.
35             Control Assoc. 23: 957-962.
36
37      Benoit, L. F.; Skelly, J. M.; Moore, L.  D.;  Dochinger, L. S. (1983) The influence of ozone on Pinus strobus
38             L. pollen germination. Can.  J. For. Res.  13: 184-187.
39
40      Berrang, P.; Karnosky, D. F.; Mickler,  R. A.; Bennet, J. P.  (1986) Natural selection for ozone tolerance in
41             Populus tremuloides. Can. J. For.  Res. 16: 1214-1216.
42
43      Berrang, P.; Karnosky, D. F.; Bennett, J.  P. (1989) Natural selection for ozone tolerance in Populus
44             tremuloides: field verification. Can. J. For. Res.  19: 519-522.
45
46      Berrang, P.; Karnosky, D. F.; Bennett, J.  P. (1991) Natural selection for ozone tolerance in Populus
47             tremuloides: an evaluation of nationwide trends. Can. J. For. Res. 21: 1091-1097.
48
49      Berry, C. R. (1964) Differences in concentrations of surface oxidant between valley and mountaintop conditions
50             in the southern Appalachians. J.  Air  Pollut. Control Assoc. 14: 238-239.
51
52      Beyers, J. L.; Riechers, G. H.; Temple, P. J. (1992) Effects  of long-term ozone exposure and drought on  the
53             photosynthetic capacity of ponderosa  pine  (Pinus ponderosa Laws.). New Phytol. 122: 81-90.
54


         December 1993                               5-356       DRAFT-DO NOT QUOTE OR CITE

-------
  1     Billen, N.; Schaetzle, H.; Seufert, G.; Arndt, U. (1990) Performance of some growth variables. Environ. Pollut.
  2            68: 419-434.
  3
  4     Bingham, G. E.; Coyne, P. I. (1977) A portable, temperature-controlled, steady-state porometer for field
  5            measurements of transpiration and photosynthesis. Photosynthetica 11: 148-160.
  6
  7     Binkley, D.; Droessler, T. D.; Miller, J. (1992) Pollution impacts at the stand and ecosystem levels. In: Olson,
  8            R. K.; Binkley, D.; Bohm, M., eds. The responses of western forests to air pollution. New York, NY:
  9            Springer Verlag; pp. 235-258 (Ecological studies no. 97).
 10
 11     Bisessar, S. (1982) Effect of ozone, antioxidant protection, and early blight on potato in the field. J. Am. Soc.
 12            Hortic. Sci.  107: 597-599.
 13
 14     Bisessar, S.; Palmer, K. T. (1984) Ozone, antioxidant spray and Meloidogyne hapla effects on tobacco. Atmos.
 15            Environ. 18: 1025-1027.
 16
 17     Bisessar, S.; Temple, P. J. (1977) Reduced ozone injury on virus-infected tobacco in the field. Plant Dis. Rep.
 18            61: 961-963.
 19
 20     Bishop, R.  C.; Welsh, M. P. (1992) Existence values in benefit-cost analysis and damage assessments. Land
 21            Econ. 68: 405-417.
 22
 23     Bishop, R.  C.; Woodward, R. T. (1993) Efficiency and sustainability in imperfect market systems. Presented at:
 24            Lessons from the ecosystem valuation forum: annual meeting of the Allied Social Sciences Association;
 25            January;  Anaheim, CA.
 26
 27     Blank, L. W.; Payer, H. D.; Pfirrmann, T.; Gnatz, G.; Kloos, M.; Runkel, K.-H.; Schmolke, W.; Strube,  D.;
 28            Rehfuess, K. E. (1990a) Effects of ozone, acid mist and soil characteristics on clonal Norway spruce
 29            (Picea ables (L.) Karst.)—an introduction to the joint 14 month tree exposure experiment in closed
 30            chambers. Environ. Pollut. 64:  189-207.
 31
 32     Blank, L. W.; Payer, H. D.; Pfirrmann, T.; Rehfuess, K. E. (1990b) Effects of ozone, acid mist and soil
 33            characteristics on clonal Norway spruce (Picea abies (L.) Karst.)—overall results and conclusions of the
 34            the joint  14 month tree exposure experiment in closed chambers. Environ. Pollut. 64: 385-395.
 35
 36     Blaschke, H.; Weiss, M. (1990) Impact of ozone, acid mist and soil characteristics on growth and development
 37            of fine roots and ectomycorrhiza of young clonal Norway spruce. Environ. Pollut. 64: 255-263.
 38
 39     Blum, U.;  Tingey, D. T. (1977) A study of the potential ways in which ozone could reduce root growth and
 40            nodulation of soybean. Atmos. Environ. 11: 737-739.
 41
 42     Blum, U.;  Heagle, A. S.;  Burns, J. C.; Linthurst, R. A. (1983) The effects of ozone on fescue-clover forage:
 43            regrowth, yield and quality. Environ. Exp. Bot. 23: 121-132.
 44
 45     Blumenthaler, M.; Ambach, W. (1990)  Indication of increasing solar ultraviolet-B radiation flux in alpine
 46            regions.  Science (Washington, DC) 248: 206-208.
 47
 48     Bogaty, H.; Campbell,  K.  S.; Appel, W. D. (1952) The oxidation of cellulose by ozone in small concentrations.
49            Text. Res. J. 22: 81-83.
50
51     Bohm, M.  (1992) Air quality and deposition. In: Olson, R. K.; Binkley, D.; Bohm, M., eds. The responses of
52            western forests  to air pollution. New York, NY: Springer Verlag; pp. 63-152 (Ecological studies no. 97).
•J J
         December  1993                               5.357       DRAFT-DO NOT QUOTE OR CITE

-------
 1     Bohm, M.; McCune, B.; Vandetta, T. (1991) Diurnal curves of troposheric ozone in the western United States.
 2             Atmos. Environ. Part A 25: 1577-1590.
 3
 4     Bolsinger, M.; Lier, M. E.; Lansky,  D.  M.; Hughes, P. R. (1991) Influence of ozone air pollution on
 5             plant-herbivore interactions. Part I: Biochemical changes in ornamental milkweed (Asclepias curassavica
 6             L.; Asclepiadaceae) induced by ozone.  Environ. Pollut. 72: 69-83.
 7
 8     Bolsinger, M.; Lier, M. E.; Hughes,  P.  R. (1992) Influence of ozone air pollution on plant-herbivore
 9             interactions. Part 2: effects of ozone on feeding preference, growth and consumption rates of monarch
10             butterflies (Danaus plexippus). Environ. Pollut. 77: 31-37.
11
12     Booker, F. L.; Fiscus, E. L.; Miller, J.  E. (1991) Ozone-induced changes in soybean cell wall physiology.
13             In: Pell, E.  J.; Steffen, K. L., eds. Active oxygen/oxidative stress and plant metabolism: proceedings,
14             6th annual Penn State Symposium in plant physiology;  May; State College, PA. Rockville, MD:
15             American Society of Plant Physiologists; pp. 229-232.  (Current topics in plant physiology: v. 6).
16
17     Booker, F. L.; Miller, J. E.; Fiscus,  E.  L. (1992) Effects of ozone and UV-B radiation on pigments, biomass
18             and peroxidase activity in soybean. In:  Berglund,  R. L., ed. Tropospheric ozone and the environment II:
19             effects, modeling and control: papers from the international specialty conference; November; Atlanta,
20             GA. Pittsburgh, PA: Air & Waste Management Association; pp. 489-503. (A&WMA transactions series:
21             no. 20).
22
23     Botkin, D. B.; Smith, W. H.; Carlson, R. W. (1971) Ozone suppression of white pine net photosynthesis. J. Air
24             Pollut. Control Assoc. 21: 778-780.
25
26     Botkin, D. B.; Smith, W. H.; Carlson, R. W.; Smith, T. L. (1972) Effects of ozone on white pine saplings:
27             variation in inhibition and recovery of net photosynthesis. Environ. Pollut. 3: 273-289.
28
29     Boutton, T. W.; Flagler, R. B. (1990) Growth and water-use efficiency of shortleaf pine as affected by ozone
30             and acid rain. Presented at: 83rd annual meeting of the Air and Waste Management Association; June;
31             Pittsburgh,  PA. Pittsburgh, PA:  Air and Waste Management Association; paper no. 90-187.7.
32
33     Braden, J. B.; Kolstad, C. D., eds. (1991) Measuring the demand for environmental quality. New York, NY:
34             Elsevier Science Publishers.
35
36     Bradley, C. E.;  Haagen-Smit, A. J. (1951) The application of  rubber in the quantitative determination of ozone.
37             Rubber Chem. Technol.  24: 750-755.
38
39     Bradshaw, A. D.; McNeilly, T.  (1991) Evolution in relation to environmental stress. In: Taylor, G. E., Jr.;
40             Pitelka,  L.  F.; Clegg, M. T., eds. Ecological genetics and air pollution. New York, NY:
41             Springer-Verlag; pp. 11-31.
42
43     Brasher, E. P.;  Fieldhouse, D. J.;  Sasser, M. (1973) Ozone injury in potato variety trials. Plant Dis. Rep.
44             57: 542-544.
45
46    Braun, S.; Fliickiger, W. (1989) Effect of ambient ozone and acid mist on aphid development. Environ. Pollut.
47            56: 177-187.
48
49     Brennan, E.;  Leone, I.  A.; Daines, R. H. (1964) The importance of variety in ozone plant damage. Plant Dis.
50            Rep.  48: 923-924.
51
52     Brennan, E.;  Leone, I.; Greenhalgh, B.; Smith, G. (1987) Chlorophyll content of soybean foliage in relation to
53            seed yield and ambient ozone pollution. JAPCA 37:  1429-1433.
54


         December 1993                                5-358       DRAFT-DO NOT QUOTE  OR CITE

-------
  1     Brennan, E. G.; Clarke, B. B.; Greenhalgh-Weidmar,  B.; Smith, G.  (1990) An assessment of the impact of
  2            ambient ozone on field-grown crops in New Jersey using the  EDU method: part 2—soybean (Glycine max
  3            (L.) Merr.). Environ. Pollut. 66: 361-373.
  4
  5     Brewer, P. F.; Heagle, A. S. (1983) Interactions between Glomus geosporum and exposure of soybeans to ozone
  6            or simulated acid rain in the field. Phytopathology 73: 1035-1040.
  7
  8     Brewer, R. F.; Guillemet, F. B.; Creveling,  R. K. (1961) Influence of N-P-K fertilization on incidence and
  9            severity of oxidant injury to mangels and spinach. Soil Sci. 92: 298-301.
 10
 11     Brookshire, D. S.; Neill, H. R.  (1992) Benefit transfers: conceptual and empirical issues. Water Resour. Res.
 12            28: 651-655.
 13
 14     Brown, T. C. (1984) The concept of value in resource allocation. Land Econ. 60: 231-246.
 15
 16     Brown, K. A.; Roberts, T. M. (1988) Effects of ozone on foliar leaching in Norway spruce (Picea abies L.
 17            Karst): confounding factors due to NOX production during ozone generation. Environ. Pollut. 55: 55-73.
 18
 19     Brown, K. A.; Roberts, T. M.; Blank, L. W. (1987) Interaction between ozone and cold sensitivity in Norway
 20            spruce: a factor contributing to the forest decline in central  Europe? New  Phytol. 105: 149-155.
 21
 22     Brown, V. C.; McNeill, S.; Ashmore, M. R. (1992) The effects of ozone fumigation on the performance of the
 23            black bean aphid, Aphis Fabae Scop., feeding on broad beans, Viciafaba L.  Agric. Ecosyst. Environ.
 24            38: 71-78.
 25
 26     Brubaker, L. B.; Vega-Gonzalez, S.; Ford, E. D.; Ribic, C. A.; Earle, C. J.; Segura,  G. (1992) Old-growth
 27            Douglas fir in western Washington. In: Olson,  R. K.; Binkley, D.; Bohm, M., eds. The responses  of
 28            western forests to air pollution. New  York, NY: Springer Verlag; pp. 333-364  (Ecological studies
 29            no. 97).
 30
 31     Bruhl, C.; Crutzen, P. J. (1989) On the disproportionate role of tropospheric ozone as  a filter against solar UV-B
 32            radiation. Geophys. Res. Lett. 16: 703.
 33
 34     Bruhn,  J. N. (1980)  Effects of oxidant air pollution on ponderosa and Jeffrey pine foliage decomposition [Ph.D.
 35            dissertation]. Berkeley, CA: University of California. Available from: University Microfilms, Ann
 36            Arbor, MI; publication no. 82-00036.
 37
 38     Butler,  L. K.; Tibbitts, T. W.; Bliss, F. A. (1979) Inheritance of resistance to ozone in Phaseolus vulgaris
 39            L. J. Am. Soc. Hortic. Sci.  104:  211-213.
 40
 41     Byres, D. P.;  Dean,  T. J.; Johnson, J. D. (1992a) Long-term effects  of ozone and simulated acid rain on the
 42            foliage dynamics of slash pine (Pinus elliottii var elliottii Engelm.). New Phytol. 120: 61-67.
 43
 44     Byres, D. P.;  Johnson, J.  D.; Dean, T. J. (1992b) Seasonal response of slash pine (Pinus elliottii var. elliottii
 45            Engelm.) photosynthesis  to long-term exposure to ozone and acidic precipitation. New Phytol.
 46            122: 91-96.
 47
 48     Bytnerowicz, A.; Olszyk, D. M.; Fox, C. A.; Dawson, P.  J.; Kats, G.; Morrison, C.  L.; Wolf, J. (1988)
49            Responses of desert annual plants to ozone and water stress in an in situ experiment. JAPCA
50            38: 1145-1151.
51
52     Bytnerowicz, A.; Poth, M.; Takemoto, B. K.  (1990) Effects of photochemical smog and mineral nutrition on
53            ponderosa pine seedlings. Environ. Pollut. 67: 233-248.
54


         December  1993                               5.359       DRAFT-DO NOT QUOTE OR  CITE

-------
 1      Callaway, J. M.; Darwin, R. F.; Neese, R. J.  (1985) Economic valuation of acidic deposition: preliminary
 2             results from the 1985 NAPAP assessment. Richland, WA: U.S. Environmental Protection Agency,
 3             National Acid Precipitation Assessment Program.
 4
 5      Cameron, J. W. (1975) Inheritance in sweet corn for resistance to acute ozone injury. J. Am. Soc. Hortic. Sci.
 6             100: 577-579.
 7
 8      Cameron, J. W.; Taylor, O. C. (1973) Injury to sweet com inbreds and hybrids by air pollutants in the field and
 9             by ozone treatments in  the greenhouse. J. Environ. Qual. 2: 387-389.
10
11      Campbell, G. G.; Schurr, G. G.; Slawikowski, D. E.; Spence, J. W. (1974) Assessing air pollution damage to
12             coatings. J. Paint Technol. 46: 59-71.
13
14      Cape, J. N.; Unsworth, M. H.  (1988) Deposition, uptake and  residence of pollutants. In: Schulte-Hostede, S.;
15             Darrall, N. M.; Blank, L. W.; Wellburn, A. R., eds.  Air pollution and plant metabolism. London.
16             United Kingdom: Elsevier Applied Science;  pp. 1-18.
17
18      Carson, R. T. (1991) Constructed markets.  In: Measuring the  demand for environmental quality. Brade, J. B.;
19             Kolstad, C. S., eds. New York, NY: Elsevier Science Publishers.
20
21      Carter,  G. A.; Mitchell, R. J.; Chappelka,  A.  H.; Brewer, C. H. (1992) Response of leaf spectral reflectance in
22             loblolly pine to increased atmospheric ozone and precipitation acidity. J. Exp. Bot. 43: 577-584.
23
24      Cass, G. R. (1991) Deterioration of materials due to ozone exposure: current problems and future research
25             needs. In: Berglund, R. L.; Lawson, D. R.; McKee, D. J., eds. Tropospheric ozone and the
26             environment: papers from an international conference;  March 1990; Los Angeles, CA. Pittsburgh, PA:
27             Air & Waste Management Association; pp. 311-320. (A&WMA transaction series no. TR-19).
28
29      Cass, G. R.; Nazaroff, W. W.; Tiller, C.;  Whitmore,  P. M. (1991) Protection of works of art from damage due
30             to atmospheric ozone. Atmos. Environ. Part A 25: 441-451.
31
32      Castle,  E. N. (1993)  A pluralistic, pragmatic and evolutionary approach to natural resource management.  For.
33             Ecol. Manage. 56: 279-295.
34
35      Castle,  E. N.; Berrens, R. P. (1993) Endangered species, economic analysis and the safe minimum standard.
36             Northwest Environ. J.: in press.
37
38      Cathey, H. M.; Heggestad, H. E. (1072) Reduction of ozone damage to Petunia hybrida Vilm. by use of growth
39             regulating chemicals and tolerant cultivars. J. Am. Soc. Hortic. Sci. 97: 695-700.
40
41      Cathey, H. M.; Heggestad, H. E. (1982) Ozone sensitivity of woody plants: modification by ethylenediurea.
42             J. Am. Soc. Hortic. Sci. 107: 1042-1045.
43
44      Chameides,  W. L. (1989) The  chemistry of ozone deposition to plant leaves: role of ascorbic acid. Environ.
45             Sci. Technol.  23: 595-600.
46
47      Chapin, F. S., Ill; Bloom, A. J.; Field, C. B.; Waring, R. H. (1987) Plant responses to multiple environmental
48             factors. BioScience 37: 49-57.
49
50      Chappelka, A. H.; Flagler, R.  B.  (1991) Future directions in ozone forestry research. In: Berglund, R. L.;
51             Lawson, D. R.; McKee, D. J., eds. Tropospheric ozone and the environment: papers from an
52             international conference; March 1990; Los Angeles, CA. Pittsburgh, PA: Air & Waste Management
53             Association; pp. 321-338. (A&WMA transaction series no. TR-19).
54


         December 1993                               5-360       DRAFT-DO NOT QUOTE OR  CITE

-------
  1     Chappelka, A. H., Ill; Chevone, B. I.; Burk, T. E. (1985) Growth response of yellow-poplar (Liriodendron
  2            tulipifera L.) seedlings to ozone, sulfur dioxide, and simulated acidic precipitation, alone and in
  3            combination. Environ. Exp. Bot. 25: 233-244.
  4
  5     Chappelka, A. H.; Chevone,  B. I.; Burk, T. E. (1988a) Growth response of green and white ash seedlings to
  6            ozone, sulfur dioxide, and simulated acid rain. For. Sci. 34: 1016-1029.
  7
  8     Chappelka, A. H.; Chevone,  B. I.; Seiler, J. R. (1988b) Growth and physiological responses of yellow-poplar
  9            seedlings exposed to ozone and simulated acidic rain. Environ. Pollut. 49: 1-18.
 10
 11     Chappelka, A. H.; Kraemer,  M. E.; Mebrahtu, T.; Rangappa, M.; Benepal, P. S.  (1988c) Effects of ozone on
 12            soybean resistance to  the Mexican bean beetle (Epilachna varivestis Mulsant). Environ. Exp. Bot.
 13            28: 53-60.
 14
 15     Chappelka, A. H.; Kush, J. S.; Meldahl, R. S.; Lockaby, B. G. (1990) An ozone-low temperature interaction in
 16            loblolly pine (Pinus taeda L.). New Phytol. 114: 721-726.
 17
 18     Chappelka, A. H.; Hildebrand,  E.; Skelly, J. M.; Mangis, D.; Renfro, J. R. (1992) Effects of ambient ozone
 19            concentrations on mature eastern hardwood trees growing in Great Smoky Mountains National Park and
 20            Shenandoah National  Park.  Presented at: 85th annual meeting of the Air and Waste Management
 21            Association; June; Kansas City, MO. Pittsburgh, PA: Air and Waste Management Association; paper
 22            no. 92-150.04.
 23
 24     Chevrier, N.; Sarhan, F.; Chung, Y. S. (1988) Oxidative damages and repair in Euglena gracilis exposed to
 25            ozone. I. SH groups and lipids. Plant Cell Physiol. 29: 321-327.
 26
 27     Chevrier, N.; Chung, Y. S.;  Sarhan, F. (1990) Oxidative damages and repair in Euglena gracilis exposed to
 28            ozone. Plant Cell Physiol. 31: 987-992.
 29
 30     Cibrian-Tovar, D. (1989) Air pollution and  forest decline near  Mexico City. Environ. Mon. Assess. 12-49-58.
 31
 32     Ciesla, W. M.; Macias-Samano, J.  (1987) Desierto de los Leones: a forest in crises. Am. Sci. 93: 29-31, 72-74.
 33
 34     Ciriacy-Wantrup, S. V.  (1952) Resource conservation: economics and policies. Berkeley, CA: University of
 35            California Press.
 36
 37     Clark, C. S.; Weber, J.  A.; Hogsett, W. E. (1993) Differential effects of ozone on photosynthesis of ponderosa
 38            pine due to needle age and position. Tree Physiol.: submitted.
 39
 40     Clarke, B. B.; Greenhalgh-Weidman, B.; Brennan, E. G. (1990) An assessment of the impact of ambient ozone
 41            on field-grown crops in  New Jersey  using the EDU method: part  1—white potato (Solarium tuberosurri).
 42            Environ. Pollut. 66: 351-360.
 43
 44     Clayberg, C. D. (1971)  Screening tomatoes  for ozone resistance. HortScience 6: 396-397.
 45
 46     Coleman, J. S.; Jones, C. G.  (1988) Plant stress and insect performance:  cottonwood, ozone and a leaf beetle.
 47            Oecologia 76: 57-61.
 48
49     Coleman, J. S.; Jones, C. G.; Smith, W. H. (1987) The effect  of ozone on cottonwood—leaf rust interactions:
50            independence of abiotic stress, genotype, and leaf ontogeny. Can. J. Bot. 65: 949-953.

52     Coleman, J. S.; Jones, C. G.; Smith, W. H. (1988) Interactions between an acute ozone  dose, eastern
53            cottonwood, and Marssonina leaf spot: implications for pathogen community dynamics. Can. J. Bot.
54            66: 863-868.


         December  1993                               5.351        DRAFT-DO NOT QUOTE OR CITE

-------
 1     Coles, J. (1993) In preparation.
 2
 3     Colls, J. J.; Unsworth, M. H. (1992) Air pollution interactions with natural stressors. In: Barker, J. R.; Tingey,
 4             D. T., eds. Air pollution effects on biodiversity. New York, NY: Van Nostrand Reinhold; pp. 93-108.
 5
 6     Common, M.; Perrings, C. (1992) Towards an ecological economics of sustainability. Ecol. Econ. 6:  7-34.
 7
 8     Cook, L. M.; Wood, R. J. (1976) Genetic effects of pollutants; environmental review: 5. Biologist 23: 129-139.
 9
10     Cooley, D. R.; Manning, W. J.  (1987) The impact of ozone on assimilate partitioning in plants: a review.
11             Environ. Pollut. 47: 95-113.
12
13     Cooley, D. R.; Manning, W. J.  (1988) Ozone effects on growth and assimilate partitioning in alfalfa,  Medicago
14             sariva L. Environ. Pollut. 49: 19-36.
15
16     Costanza, R. (1991) Assuring sustainability of ecological economic systems. In: Costanza,  R., ed. Ecological
17             economics: the science and management of sustainability. New York, NY: Columbia University Press.
18
19     Costanza, R.; Daly, H. E.; Bartholomew, J. A. (1991) Goals, agendas and policy recommendations for
20             ecological economics. In: Costanza, R., ed. Ecological economics: the science and management of
21             sustainability. New York, NY: Columbia University Press.
22
23     Costonis,  A. C.; Sinclair,  W. A. (1972) Susceptibility of healthy and ozone-injured needles of Pinus strobus to
24             invasion by Lophodermium pinastri and Aureobasidium pullulans. Eur. J. For. Pathol. 2: 65-73.
25
26     Cowling,  D. W.; Koziol, M. J.  (1982) Mineral nutrition and plant response to air pollutants. In: Unsworth,
27             M. H.; Ormrod, D. P.,  eds. Effects of gaseous air pollution on agriculture and horticulture. London,
28             United Kingdom: Butterworth Scientific; pp. 349-375.
29
30     Cox, R. M.; Spavold-Tims, J.; Hughes, R. N, (1989)  Acid fog and ozone: their possible role in birch
31             deterioration around the Bay of Fundy, Canada. Water Air Soil Pollut. 48: 263-276.
32
33     Crabtree, J.; Malm, F. S. (1956) Deterioration of rubber from use and with age.  In: McPherson, A. T.; Klemin,
34             A., eds. Engineering uses of rubber. New York, NY: Reinhold Publishing Corp.;  pp. 140-170.
35
36     Cregg,  B. M.;  Halpin, J. E.; Dougherty, P. M.; Testey, R. O. (1989) Comparative physiology and morphology
37             of seedling and mature forest^trees. In: Noble, R. D.; Martin, J. L.; Jensen, K. F., eds. Air pollution
38             effects  on vegetation including forest ecosystems. Washington, DC: U.S. Department of Agriculture,
39             Northeastern Experiment Station; pp. 111-118.
40
41     Crocker, T. D. (1985a) On the value of the condition  of a forest stock. Land Econ. 61: 244-254.
42
43      Crocker,  T. D. (1985b) Economy impact of acid rain. Statement before Select Committee on Small Business and
44            Committee on Environment and Public Works. U.S. Senate; September 23.
45
46     Crocker,  T. D. (1993) Ecosystem functions, economics, and the ability to function. In: Milton, J. W.; Shogren,
47            J.; Young, M., eds. Integrating economic and ecological indicators: proceedings of the symposium of the
48            Resource Policy Consortium; May; Washington, D.C.
49
50     Crocker,  T. D.; Forster, B. A.  (1985) Some economic implications of the alternative biological and chemical
51             explanations of the impacts of acid deposition  on forest ecosystems. Presented at:  international
52            symposium on acidic deposition; Muskoka, Canada.
53
          December 1993                               5-362       DRAFT-DO NOT QUOTE OR CITE

-------
  1      Gumming, J. R.; Alscher, R. G.; Chabot, J.; Weinstein, L. H. (1988) Effects of ozone on the physiology of red
  2             spruce seedlings. In: Proceedings of the US/FRG research symposium: effects of atmospheric pollutants
  3             on the spruce-fir forests of the eastern United States and the Federal Republic of Germany. USDA Forest
  4             Service, Northeastern Forest Experiment Station; pp. 355-363; general technical report no. NE-120.
  5
  6      Cure, W. W.; Sanders,  J. S.; Heagle, A. S. (1986) Crop yield response predicted with different characterizations
  7             of the same ozone treatments. J. Environ. Qual. 15: 251-254.
  8
  9      Dahlsten, D. L.; Rowney, D. L. (1980) Influence of air pollution on population dynamics of forest insects and on
10             tree mortality. In: Miller, P. R., ed. Proceedings of the symposium on effects of air pollutants on
11             Mediterranean and temperate forest ecosystems; June; Riverside, CA. Berkeley, CA: U.S. Department of
12             Agriculture, Pacific Southwest Forest and Range Experiment Station; pp. 125-130; Forest Service general
13             technical report  no. PSW-43. Available from: NTIS, Springfield, VA; PB81-133720.
14
15      Daines, R. H.; Leone, I. A.; Brennan,  E. (1960) Air pollution as it affects agriculture in New Jersey. New
16             Brunswick, NJ:  New Jersey  Agricultural Experiment Station, Rutgers; bulletin no.  794.
17
18      Damicone, J. P.; Manning, W. J.; Herbert,  S. J.; Feder, W. A. (1987a) Growth and disease response of
19             soybeans from early maturity groups to ozone and Fusarium oxysporum. Environ. Pollut. 48: 117-130.
20
21      Damicone, J. P.; Manning, W. J.; Herbert,  S. J.; Feder, W. A. (1987b) Foliar sensitivity of soybeans from
22             early maturity groups to ozone and inheritance  of injury response. Plant Dis. 71: 332-336.
23
24      Dann, M. S.; Pell, E. J. (1989) Decline of activity and quantity of ribulose bisphosphate carboxylase/oxygenase
25             and net photosynthesis in ozone-treated potato foliage. Plant Physiol. 91: 427-432.
26
27      Darley, E. F.; Kettner,  K. A.; Stephens, E. R. (1963)  Analysis of peroxyacyl nitrates by gas chromatography
28             with electron capture detection. Anal. Chem. 35: 589-591.
29
30      Darrall, N. M. (1989) The effect of air pollutants on physiological processes in plants.  Plant Cell Environ.
31             12: 1-30.
32
33      Dassel, K. A.; Rawlings, J.  O. (1988) Experimental design strategy for the Weibull dose response model.
34             Environ. Pollut. 53: 333-349.
35
36      Davidson, A. (1993) Update of ozone trends in California's South Coast Air Basin.  Air Waste 43: 226-227.
37
38      Davidson, S. R.; Ashmore, M. R.; Garretty, C. (1992) Effects of ozone and water deficit on the growth and
39             physiology of Fagus sylvatica. For.  Ecol. Manage. 51: 187-193.
40
41      Davies, K. M.  (1979) Influence of environmental factors on interply adhesion. In: Proceedings of the
42             international rubber conference; pp.  80-89.
43
44      Davies, W. J.;  Zhang, J. (1991) Root signals and the regulation of growth and development of plants in drying
45             soil. Annu. Rev. Plant Physiol. Plant Mol. Biol. 42: 55-76.
46
47      Davies, W. J.;  Mansfield, T. A.;  Wellburn, A. R. (1980) A role for abscisic acid in drought endurance and
48             drought avoidance. In: Skoog, F., ed.  Plant growth substances 1979: proceedings of the 10th
49             international conference on plant growth substances; July  1979; Madison, WI. New York, NY:
50             Springer-Verlag; pp. 242-253.
51
52      Davis, D. D.; Kress, L. (1974) The relative susceptibility of ten bean varieties to ozone. Plant Dis. Rep.
53             58: 14-16.
54


         December  1993                               5.353        DRAFT-DO NOT QUOTE OR CITE

-------
  1      Davis, D. D.; Skelly, J. M. (1992a) Growth response of four species of eastern hardwood tree seedlings exposed
  2             to ozone, acidic precipitation, and sulfur dioxide. J. Air Waste Manage. Assoc. 42: 309-311.
  3
  4      Davis, D. D.; Skelly, J. M. (1992b) Foliar sensitivity of eight eastern hardwood tree species to ozone. Water Air
  5             Soil Pollut. 62: 269-277.
  6
  7      Davis, D. D.; Hutnik, R. J.; McClenahen, J. R. (1993) Evaluation of vegetation near coal-burning power plants
  8             in southwestern Pennsylvania. II. Ozone injury on foliage of hybrid poplar. Air Waste 43: 760-764.
  9
10      Davison, A. W.; Barnes, J.  D.; Renner, C. J. (1988) Interactions between air pollutants and cold stress.
11             In: Schulte-Hostede, S.; Darrall, N. M.; Blank, L. W.; Wellburn, A. R., eds. Air pollution and plant
12             metabolism. London, United Kingdom: Elsevier Applied Science; pp. 307-328.
13
14      De Santis, F.; Di Palo, V.; Allegrini, I. (1992) Determination of some atmospheric pollutants inside a museum:
15             relationship with the concentration outside. Sci. Total Environ. 127: 211-223.
16
17      De Temmerman, L.; Vandermeiren, K.; Guns, M. (1992) Effects of air  filtration on spring wheat grown in
18             open-top field chambers as a rural site I. effect on growth yield and dry matter partitioning. Environ.
19             Pollut. 77: 1-5.
20
21      De Vos, N. E.;  Hill, R. R., Jr.; Pell, E. J.;  Cole, R. H. (1982) Quantitative inheritance of ozone resistance in
22             potato. Crop Sci. 22: 992-995.
23
24      Dean, T. J.; Johnson, J. D.  (1992) Growth response of young slash pine trees to simulated acid rain and ozone
25             stress. Can. J. For. Res. 22: 839-848.
26
27      Decoteau, D.  R.; Grant, L.; Craker, L. E. (1986) Failure of ozone susceptibility tests to predict yield reductions
28             in wheat. Field Crops Res. 13:  185-191.
29
30      DeHayes, D. H.; Thornton, F. C.; Waite, C. E.; Ingle, M. A. (1991) Ambient cloud deposition reduces cold
31             tolerance of red spruce seedlings. Can. J. For. Res. 21:  1292-1295.
32
33      Deveau, J. L.; Ormrod, D. P.; Allen, O. B.; Beckerson, D. W. (1987)  Growth and foliar injury responses of
34             maize, soybean and tomato seedlings exposed to mixtures of ozone and sulphur dioxide. Agric. Ecosyst.
35             Environ. 19: 223-240.
36
37      Diaz, H. F.; Bradley, R. S.; Eischeid,  J. K. (1989) Precipitation fluctuations over global land areas since the late
38             1800's. J. Geophys. Res.  94: 1195-1210.
39
40      Dickson, R. E.; Isebrands, J. G. (1991) Leaves as regulators of stress response. In: Mooney, H. A.; Winner,
41             W. E.; Pell, E. J., eds. Response of plants to multiple stresses.  San Diego, CA: Academic Press, Inc.;
42             pp. 3-34.
43
44      Dimauro, P. J.; Paris, H. L.; Path, M. A. (1979) Wax protection. Rubber Chem. Technol. 52: 973-984.
45
46      Dobson, M. C.; Taylor, G.; Freer-Smith, P. H. (1990) The control of ozone uptake by Picea abies (L.) Karst.
47             and P. sitchensis (Bong.) Carr. during drought and interacting effects on shoot water relations. New
48             Phytol.  116: 465-474.
49
50      Dochinger, L. S.; Townsend, A.  M. (1979)  Effects of roadside deicer salts and ozone on red maple progenies.
51             Environ. Pollut. 19: 229-237.
52
53      Dohmen, G. P.  (1987) Secondary effects of air pollution: ozone decreases brown rust disease potential in wheat.
54             Environ. Pollut. 43: 189-194.


         December 1993                               5-364       DRAFT-DO NOT QUOTE OR  CITE

-------
  1     Dohmen, G. P.  (1988a) Is plant resistance to air pollution related to plant resistance towards disease?
  2            In: A report from the Commission of the European Communities; pp.  158-162.
  3
  4     Dohmen, G. P.  (1988b) Indirect effects of air pollutants: changes in plant/parasite interactions. Environ. Pollut.
  5            53: 197-207.
  6
  7     Dohmen, G. P.; Koppers, A.; Langebartels, C. (1990) Biochemical response of Norway spruce (Picea abies (L.)
  8            Karst.) towards 14-month exposure to ozone and acid mist: effects of amino acid, glutathione and
  9            polyamine liters. Environ. Pollut. 64:  375-383.
 10
 11     Donnelly, D. M.; Sorg-Swanson,  C.; Loomis, J. B.; Nelson, L. J. (1990) Net economic value of hunting and
 12            fishing in Idaho.  In: Vining, J., ed. Social science and natural resource recreation management. Boulder,
 13            CO:  Westview Press; pp.  257-279 (Field, D. R., ed.  Social behavior and natural resources series).
 14
 15     Dorset, B. C. M. (1972) Pollution and fading fabrics. Text. Manuf. 99: 27-29.
 16
 17     Doss, C. R.; Taff, S. J.  (1993) The relationship of property values and wetlands proximity in Ramsey County,
 18            Minnesota. Minneapolis, MN: University of Minnesota, Department of Applied Economics; economic
 19            report 93-4.
 20
 21     Dowding, P. (1988) Air pollutant effects on plant pathogens. In: Schulte-Hostede, S.; Darrall, N. M.; Blank,
 22            L. W.; Wellburn, A. R., eds. Air pollution and plant metabolism. London, United Kingdom: Elsevier
 23            Applied Scientific; pp. 329-355.
 24
 25     Dragoescu, N.; Hill, R. R., Jr.; Pell, E. J. (1987) An autotetraploid model for genetic analysis of ozone
 26            tolerance in potato, Solatium tuberosum L. Genome 29: 85-90.
 27
 28     Druzik, J. R.; Adams, M. S.; Tiller, C.;  Cass, G. R. (1990)  The measurement and model predictions of indoor
 29            ozone concentrations hi museums. Atmos. Environ. Part A 24: 1813-1823.
 30
 31     Dueck, Th. A.;  Dil, E. W.; Pasman, F. J. M. (1987) Adaptation of grasses in the Netherlands to air pollution.
 32            New Phytol. 108: 167-174.
 33
 34     Duffield, J. H. (1989) RPA values for recreation: theory and  practice. Public Land Law Rev. 10:  105-130.
 35
 36     Duffield, J. W.; Neher, C.  J.; Brown, T. C.  (1992) Recreation benefits of instream flow: application to
 37            Montana's Big Hole and Bitterroot rivers. Water Resour.  Res. 28: 2169-2181.
 38
 39     Dugger, W.  M., Jr.; Taylor, O. C.; Cardiff, E.; Thompson, C. R. (1962) Relationship between carbohydrate
 40            content and susceptibility of pinto bean plants to ozone damage. Proc.  Am. Soc. Hort. Sci.  81: 304-314.
 41
 42     Dunn, D. B. (1959) Some effects of air pollution on Lupinus in the Los Angeles area. Ecology 40: 621-625.
 43
44     Dunning, J. A.; Heck, W. W.;  Tingey, D. T. (1974) Foliar sensitivity of pinto bean and soybean to ozone as
45            affected  by temperature, potassium nutrition and ozone dose. Water Air Soil Pollut.  3: 305-313.
46
 47     Duriscoe, D. M. (1990) Cruise  survey of oxidant air pollution injury to Pinus ponderosa and Pinusjeffreyi in
 48            Saguaro National Monument, Yosemite National Park, and  Sequoia and Kings' Canyon National Parks.
49            Denver,  CO: National Park Service, Air Quality Division; NPS/AQD-90/003.
50
51     Duriscoe, D. M.; Stolte,  K.  W. (1989) Photochemical oxidant injury to ponderosa (Pinusponderosa Dougl.
52            ex Laws) and Jeffrey pine (Pinusjeffreyi Grev. and Balf.) in the national parks of the Sierra Nevada of
53            California. In: Olson, R. K.; Lefohn, A. S., eds. Effects of air pollution on western forests. Pittsburgh,
54            PA: Air and Waste  Management Asssociation; pp. 261-278 (Transactions series, no. 16).


         December 1993                               5.365        DRAFT-DO NOT QUOTE OR CITE

-------
 1     Eamus, D.; Murray, M. (1991) Photosynthetic and stomatal conductance responses of Norway spruce and beech
 2             to ozone, acid mist and frost—a conceptual model. Environ. Pollut. 72: 23-44.
 3
 4     Eason, G.; Reinert, R. A. (1991) Responses of closely related Bush Blue Lake snap bean cultivars to increasing
 5             concentrations of ozone. J. Am. Soc. Hortic. Sci. 116: 520-524.
 6
 7     Ebel, B.; Rosenkrantz, J.; Schiffgens, A.; Lfitz, C.  (1990) Cytological observations on spruce needles after
 8             prolonged treatment with ozone and acid mist. Environ. Pollut. 64: 323-335.
 9
10     Edinger, J. G.; McCutchan, M. H.; Miller, P. R.; Ryan, B. C.; Schroeder, M. J.; Behar, J. V. (1972)
11             Penetration and duration of oxidant air pollution in the South Coast Air Basin of California. J. Air Pollut.
12             Control Assoc. 22: 882-886.
13
14     Edmunds, R. L.; Basabe, F. A. (1989)  Ozone concentrations above a Douglas fir forest canopy in western
15             Washington, U.S.A. Atmos. Environ. 23: 625-629.
16
17     Edwards, N. T.  (1991) Root and soil respiration responses to ozone in Pinus taeda L. seedlings. New Phytol.
18             118:315-321.
19
20     Edwards, S.  F. (1992) Rethinking existence values.  Land Econ. 68: 120-122.
21
22     Edwards, G. S.; Kelly, J. M. (1992) Ectomycorrhizal colonization of loblolly pine seedlings during three
23             growing seasons in response to  ozone, acidic precipitation, and soil Mg status. Environ. Pollut.
24             76: 71-77.
25
26     Edwards, D. C.; Storey, E. B. (1959) A quantitative ozone test for small specimens. Chem. Can.  11: 34-38.
27
28     Edwards, G. S.; Pier, P. A.; Kelly, J. M. (1990a) Influence of ozone and soil magnesium status on the cold
29             hardiness of loblolly pine (Pinus taeda L.) seedlings. New Phytol. 115: 157-164.
30
31     Edwards, N. T.; Taylor, G. E., Jr.; Adams, M. B.; Simmons,  G. L.; Kelly, J. M. (1990b) Ozone, acidic rain,
32             and soil magnesium effects on growth and foliar pigments of Pinus taeda L. Tree Physiol. 6: 95-104.
33
34     Edwards, G. S.;  Edwards, N. T.; Kelly, J. M.; Mays, P. A. (1991a) Ozone, acidic precipitation,  and soil Mg
35             effects on growth and nutrition of loblolly pine seedlings. Environ. Exp. Bot. 31: 67-78.
36
37     Edwards, P. J.; Wood, F.; Kochenderfer, J. N. (1991b) Characterization of ozone during consecutive drought
38             and wet years at a rural West Virginia site.  J. Air Waste Manage. Assoc. 41: 1450-1453.
39
40    Edwards, N. T.; Edwards, G. L.; Kelly, J. M.; Taylor, G. E., Jr. (1992a) Three-year growth responses of
41             Pinus taeda L. to simulated rain chemistry, soil magnesium status, and ozone.  Water Air Soil Pollut.
42             63: 105-118.
43
44     Edwards, G. S.; Friend, A. L.; O'Neill, E. G.; Tomlinson, P. T. (1992b) Seasonal patterns of biomass
45             accumulation and carbon allocation in Pinus taeda seedlings exposed to ozone, acidic precipitation, and
46            reduced soil Mg. Can. J. For. Res. 22: 640-646.
47
48     Edwards, G. S.; Kelly, J. M.; Mays, P.  A. (1992c) Ozone, acidic precipitation and soil Mg impacts on soil and
49            loblolly pine seedling nutrient status after three growing seasons.  Water Air Soil  Pollut. 63: 281-294.
50
51     Ehleringer, J. R. (1991) Estimating costs of air pollution resistance. In: Taylor, G. E., Jr.; Pitelka, L.  F.; Clegg,
52            M. T.; eds. Ecological genetics and air pollution. New York, NY: Springer-Verlag; pp. 203-207.
53
          December  1993                               5-366       DRAFT-DO NOT QUOTE OR CITE

-------
 1     Eissenstat, D. M.; Syvertsen, J. P.; Dean, T. J.;  Yelenosky, G.; Johnson, J. D. (1991a) Sensitivity of frost
 2             resistance and growth in citrus and avocado to chronic ozone exposure. New Phytol. 118: 139-146.
 3
 4     Eissenstat, D. M.; Syvertsen, J. P.; Dean, T. J.;  Johnson, J.  D.; Yelenosky, G. (1991b) Interaction of simulated
 5             acid rain with ozone on freeze resistance, growth, and mineral nutrition in citrus and avocado. J. Am.
 6             Soc. Hortic. Sci. 116: 838-845.
 7
 8     Elkiey, T.; Ormrod, D. P.  (1979a) Leaf diffusion resistance responses of three petunia cultivars to ozone and/or
 9             sulfur dioxide. J. Air Pollut. Control Assoc. 29: 622-625.
10
11     Elkiey, T.; Ormrod, D. P.  (1979b) Petunia cultivar sensitivity to ozone and sulphur dioxide. Sci. Hortic.
12             (Amsterdam) 11: 269-280.
13
14     Elkiey, T.; Ormrod, D. P.; Pelletier, R. L. (1979)  Stomatal and leaf surface features as related to the ozone
15             sensitivity of petunia cultivars. J.  Am. Soc. Hortic. Sci. 104: 510-514.
16
17     Elliott, C. L.; Eberhardt, J. C.; Brennan, E. G. (1987) The effect of ambient ozone pollution and acidic rain on
18             the growth and chlorophyll content of green and white ash. Environ. Pollut.  44: 61-70.
19
20     Enders, G.; Dlugi, R.; Steinbrecher, R.; Clement, B.; Daiber, R.; Euk, J. V.; Gab, S.; Haziz, M.; Helas, G.;
21             Herrmann, U.; Kessel, M.; Kesselmeier,  J.; Kotzias, D.; Kurtidis, K.; Kurth, H.-H.; McJillen, R. T.;
22             Roider, G.; Schumann, W.; Teichmann, U.; Torres, L. (1992) Biosphere/atmosphere interactions:
23             integrated research  in a European coniferous forest  ecosystem. Atmos. Environ. Part A 26: 171-189.
24
25     Endress, A. G.; Post, S. L. (1985) Altered feeding preference of Mexican bean beetle Epilachna varivestis for
26             ozonated soybean foliage. Environ. Pollut. Ser. A 39: 9-16.
27
28     Engle, R. L.; Gabelman, W. H.  (1966) Inheritance and mechanism for resistance to ozone damage in onion,
29             Allium cepa L. Proc. Am. Soc. Hortic. Sci. 89: 423-430.
30
31     Ennis, C. A.; Lazrus,  A. L.; Kok, G. L.; Zimmerman, P.  R. (1990) A branch chamber system and techniques
32             for simultaneous pollutant exposure experiments and gaseous flux determinations. Tellus 42B:  170-182.
33
34     Ensing, J.; Hofstra, G.; Adomait, E. J. (1986) The use of cultivar yield data to estimate losses due to ozone in
35             peanut. Can. J. Plant Sci. 66:  511-520.
36
37     Enyedi, A. J.; Eckardt, N. A.; Pell, E. J. (1992) Activity of ribulose biphosphate carboxylase/oxygenase from
38             potato cultivars with differential response to ozone stress. New  Phytol. 122:  493-500.
39
40     Ernst, W. H. O.; Tonneijck, A.  E. C.; Pasman,  F. J. M. (1985) Ecotypic response  of Silene cucubalus to air
41             pollutants (SO2, O3). J. Plant  Physiol.  118: 439-450.
42
43     Evans, P. A.; Ashmore, M. R. (1992) The effects of ambient air on a semi-natural grassland community. Agric.
44             Ecosyst.  Environ. 38: 91-97.
45
46     Eversman, S.; Sigal, L. L. (1987) Effects of SO2, O3, and SO2 and O3 in combination on photosynthesis and
47             ultrastructure  of two lichen species. Can. J. Bot.  65:  1806-1818.
48
49     Fangmeier,  A.; Kress, L. W.; Lepper, P.; Heck, W. W. (1990) Ozone effects on the fatty acid composition of
50             loblolly pine needles (Pinus taeda L.) New Phytol. 115:  639-647.
51
52     Farquhar, G.  D.; Ehleringer, J. E.; Hubick, K. T.  (1989) Carbon  isotopic discrimination and photosynthesis.
53             Annu. Rev. Plant Physiol. 40: 503-537.
54


         December 1993                                5-367       DRAFT-DO  NOT QUOTE OR CITE

-------
 1     Feder, W. A.  (1968) Reduction in tobacco pollen germination and tube elongation, induced by low levels of
 2             ozone. Science (Washington, DC) 160:  1122.
 3
 4     Feder, W. A.  (1970) Plant response to chronic exposure of low levels of oxidant type air pollution. Environ.
 5             Pollut. 1: 73-79.
 6
 7     Feder, W. A.  (1986) Using pollen to predict species response to ozone stress. Phytopathology 76: 1097.
 8
 9     Feder, W. A.; Shrier, R. (1990) Combination of U.V.-B. and ozone reduces pollen tube growth more than either
10             stress alone. Environ. Exp. Bot. 30: 451-454.
11
12     Feder, W. A.; Sullivan, F. (1969) Differential susceptibility of pollen grains to ozone injury. Phytopathology
13             59: 399.
14
15     Federal Register. (1993) Natural resource damage assessments under the Oil Pollution Act of 1990. F. R.
16             (January 15) 58: 4601-4614.
17
18     Fenn, M. E.; Dunn, P. H. (1989) Litter decomposition across an air-pollution gradient in the San Bernardino
19             Mountains. Soil Sci. Soc. Am. J.  53: 1560-1567.
20
21     Fenn, M. E.; Dunn, P. H.; Wilborn, R. (1990) Black stain root disease in ozone-stressed ponderosa pine. Plant
22             Dis. 74: 426-430.
23
24     Fincher, J. (1992) Comparison of structural changes in red spruce (Picea rubens Sarg.) during cold hardening in
25             mature trees and  in seedlings used in  pollutant exposure studies. For.  Ecol. Manage. 51: 105-113.
26
27     Fincher, J.; Cumming, J. R.; Alscher, R. G.; Rubin, G.; Weinstein, L. (1989) Long-term ozone exposure
28             affects winter hardiness of red spruce (Picea  rubens Sarg.) seedlings. New Phytol. 113:  85-96.
29
30     Fincher, J.; Cumming, J. R.; Alscher, R. G.; Ruben, G.; Weinstein, L. (1990) Long term ozone exposure
31             affects winter hardiness of red spruce. New Phytol.
32
33     Fiscus, E. L.; Booker, F. L.; Miller, J. E.; Heagle,  A. S. (1990) Effects of enhanced tropospheric ozone and
34             UV-B irradiation on soybean. In:  Bruck, R. I., ed. Global climate change symposium proceedings; April;
35             Raleigh, NC.  Raleigh, NC: North Carolina State University, Department of Agricultural
36             Communications; pp. 26-35; bulletin 479.
37
38     Fisher, H.  L.  (1957) Antioxidation and antiozonation. In: Chemistry of natural and synthetic rubbers. New York,
39             NY: Reinhold Publishing Corporation; pp. 49-55.
40
41     Flagler, R. B.; Younger, V. B. (1982) Ozone and sulfur dioxide effects on three tall fescue cultivars. J. Environ.
42             Qual.  11: 413-416.
43
44     Flagler, R. B.; Patterson, R. P.; Heagle,  A.  S.; Heck, W. W. (1987) Crop physiology & metabolism: ozone and
45             soil moisture deficit effects on nitrogen metabolism of soybean. Crop Sci. 27: 1177-1184.
46
47     Flagler, R. B.; Barrows, C. F.; Chappelka, A. H.; Johnson, J. D.;  Kress, L. W.; Reardon, J. D.; Fox, S.
48            (1993) Combined analyses of three southern pine species exposed to ozone and acidic rain:  I. growth and
49            biomass responses. J. Environ. Qual.: submitted.
50
51      Fletcher, R. A.; Hofstra, G. (1985) Triadimefon a plant multi-protectant. Plant Cell  Physiol. 26: 775-780.
52
53     Floyd, R. A.; West, M. S.; Hogsett, W. E.; Tingey, D. T.  (1989) Increased 8-hydroxyguanine content of
54             chloroplast DNA from ozone-treated plants. Plant Physiol. 91: 644-647.


         December 1993                               5-368       DRAFT-DO  NOT QUOTE OR CITE

-------
  1      Floyd et al. (1992).
  2
  3      Fluckiger, W.; Braun, S.; Bolsinger, M. (1988) Air pollution: effect on hostplant-insect relationships.
  4             In: Schulte-Hostede, S.; Darrall, N. M.; Blank, L. W.;  Wellburn, A. R., eds. Air pollution and plant
  5             metabolism. London, United Kingdom: Elsevier Applied Science; pp. 366-380.
  6
  7      Fowler, D.; Cape, J. N. (1982) Air pollutants in agriculture and horticulture. In: Unsworth, M. H.; Ormrod,
  8             D. P., eds. Effects of gaseous air pollution in agriculture and horticulture. London, United Kingdom:
  9             Butterworth Scientific; pp. 3-26.
10
11      Foy, G. (1990) Economic sustainability and the preservation of environmental assets. Environ. Manage.
12             14: 771-778.
13
14      Fravel, D. R.; Benson, D. M.; Reinert, R.  A. (1984) Response of shore juniper to ozone alone and in mixture
15             with sulfur dioxide and nitrogen dioxide. Hortscience 19: 694-695.
16
17      Freeman, A. M., HI. (1979) The benefits of air and water pollution control: a review and synthesis of recent
18             estimates.  Washington, DC: Council on  Environmental Quality. Available from: NTIS, Springfield, VA;
19             PB80-178759.
20
21      Freer-Smith, P. H.; Dobson, M. C. (1989)  Ozone flux to Picea sitchensis (Bong) Carr. and Picea abies (L)
22             Karst during short episodes an d the effects of these on transpiration and photosynthesis. Environ. Pollut.
23             59: 161-176.
24
25      Freer-Smith, P. H.; Taylor,  G. (1992) Comparative evaluation of the effects of gaseous pollutants, acidic
26             deposition and mineral deficiencies on gas exchange of trees.  Agric. Ecosyst. Environ. 42: 321-332.
27
28      Fuentes, J. D.; Gillespie, T. J. (1992) A gas exchange system to study the effects of leaf surface wetness on the
29             deposition of ozone. Atmos. Environ. Part A 26: 1165-1173.
30
31      Fuentes, J. D.; Gillespie, T. J.; den Hartog, G.; Neumann, H. H. (1992) Ozone deposition onto a deciduous
32             forest during dry and wet conditions. Agric. For. Meteorol. 62: 1-18.
33
34      Fuhrer, J.; Egger, A.; Lehnherr, B.; Grandjean, A.; Tschannen, W.  (1989) Effects of ozone on the yield of
35             spring wheat (Triticum aestivum L., cv.  Albis) grown in open-top field chambers. Environ. Pollut.
36             60: 273-290.
37
38      Fuhrer, G.; Dunkl, M.; Knoppick, D.; Selinger, H.; Blank,  L. W.; Payer, H. D.; Lange, O. L. (1990) Effects
39             of low-level long-term ozone fumigation and acid mist on photosynthesis and stomata of clonal Norway
40             spruce (Picea abies (L.) Karst.). Environ.  Pollut. 64: 279-293.
41
42      Fuhrer, J.; Grimm, A.  G.; Tschannen, W.;  Shariat-Madari, H.  (1992) The response of spring wheat (Triticum
43             aestivum L.) to ozone at higher elevations: II. changes in yield, yield components and grain quality in
44             response to ozone flux. New Phytol. 121: 211-219.
45
46      Ganslandt, E.; Svensson, S.  (1980) Stress relaxation tests for determination of ozone attack on rubber. Polym.
47             Test. 1: 81-89.
48
49      Garcia, P.; Dixon, B.; Mjelde, J.; Adams, R.  (1986) Measuring the benefits of environmental change using a
50             duality approach: the case of ozone and Illinois cash grain farms. J. Environ. Econ. Manage. 13: 69-80.

52
         December  1993                               5_369       DRAFT-DO NOT QUOTE OR CITE

-------
  1     Gamer, J. H. B. (1991) Ozone exposure and nitrogen loading in the forests of eastern North America.
  2            In: Berglund, R. L.; Lawson, D. R.; McKee, D. J., eds. Tropospheric ozone and the environment:
  3            papers from an international conference;  March 1990; Los Angeles, CA. Pittsburgh, PA: Air & Waste
  4            Management Association; pp. 289-310. (A&WMA transaction series no. TR-19).

  6     Garner, J. H. B. (1993) Nitrogen oxides, plant metabolism, and forest ecosystem response. In: Wellburn, A., ed.
  7            Third international symposium on gaseous plants and plant metabolism; July 1992; Blacksburg,  VA.
  8            In press.
  9
10     Gamer, J. H. B.; Pagano, T.; Cowling, E. B. (1989) An evaluation of the role of ozone, acid deposition, and
11            other airborne pollutants  in the forests of eastern North America. Asheville, NC: U.S.  Department of
12            Agriculture, Forest Service, Southeastern Forest Experiment Station; general technical report SE-59.

14     Gillespie, C. T.; Winner, W. E.  (1989) Development of lines of radish differing in resistance to O3 and SO2-
15            New Phytol. 112: 353-361.
16
17     Gimeno, B. S.; Velissariou,  D.; Barnes, J.  D.; Inclan, R.; Pena, J. M.; Davison, A.  W. (1993) Ozone effects
18            on aleppo pine needles in Greece and Spain. Phytopathol. Mediterr.: submitted.
19
20     Goodyear, S. N.; Ormrod, D. P. (1988) Tomato response to concurrent and sequential NO2 and O3 exposures.
21            Environ. Pollut. 51:  315-326.
22
23     Gorissen, A.; Van Veen, J. A. (1988) Temporary disturbance of translocation of assimilates in Douglas firs
24            caused by low levels of ozone and sulfur dioxide. Plant Physiol. 88: 559-563.
25
26     Gorissen, A.; Schelling, G. C.; van Veen, J. A.  (1991a) Concentration-dependent effects of ozone on
27            translocation of assimilates  in Douglas fir. J.  Environ. Qual. 20: 169-173.
28
29     Gorissen, A.; Joosten, N. N.; Jansen, A. E. (1991b) Effects of ozone and ammonium sulphate on carbon
30            partitioning to mycorrhizal  roots of juvenile Douglas fir. New Phytol. 119:  243-250.
31
32     Graham, S.;  Ormrod, D. P.  (1989) Sorption of ozone by 'New Yorker'  tomato leaves. Environ. Pollut.
33            58: 213-220.
34
35     Grandjean, A.; Fuhrer, J. (1989) Growth and leaf senescence in spring wheat (Triticum aestivum)  grown at
36            different ozone concentrations in open-top field chambers. Physiol. Plant. 77: 389-394.
37
38     Grandjean, A. G.; Fuhrer, J. (1992a) The responses of spring wheat (Triticum aestivum L.) to ozone at higher
39            elevations. 1. Measurement of ozone and carbon dioxide fluxes in open-top field chambers. New Phytol.
40            121:  201-210.
41
42     Grandjean, A. G.; Fuhrer, J. (1992b) The response of spring wheat (Triticum aestivum L) to ozone at higher
43            elevatiohns. 3. Responses of leaf and canopy gas exchange, and  chlorophyll fluorescence to ozone flux.
44            New Phytol. 122: 122: 321-328.
45
46     Graybill, D.  A.  (1992) Coniferous  forests of the  Colorado front range. Part A: mixed species in unmanaged
47            stands. In: Olson, R. K.; Binkley, D.; Bohm, M., eds. The responses of western forests to air pollution.
48            New York, NY: Springer Verlag; pp. 370-384 (Ecological studies no. 97).
49
50     Graybill, D.  A.; Rose, M. R. (1989) Analysis of growth trends and vriation in conifers from Arizona and New
51            Mexico. In: Olson, R. K.;  Lefohn, A. S., eds. Effects of air pollution on western forests. Pittsburgh,
52            PA: Air and Waste Management  Association; pp. 261-278 (Transactions series no.  16).
53
54     Greenhut, G. K. (1983) Resistance  of a pine forest to ozone uptake. Boundary Layer Meteorol.  27: 387-391.


         December 1993                              5-370      DRAFT-DO NOT  QUOTE OR CITE

-------
 1     Gregorius, H.-R. (1989) The importance of genetic multiplicity for tolerance of atmospheric pollution.
 2            In: Scholz, F.; Gregorius, H.-R.; Rudin, D., eds. Genetic effects of air pollutants in forest tree
 3            populations: proceedings of the joint meeting of the IUFRO working parties; August 1987;
 4            Grosshansdorf, West Germany. Berlin, Germany: Springer-Verlag; pp. 163-172.
 5
 6     Greitner, C. S.; Winner, W. E. (1988) Increases in 613C values of radish and soybean plants caused by ozone.
 7            New Phytol. 108: 489-494.
 8
 9     Greitner, C. S.; Winner, W. E. (1989) Effects of O3 on alder photosynthesis and symbiosis with Frankia. New
10            Phytol. Ill: 647-656.
11
12     Grime, J. P. (1979) Plant strategies and vegetation processes. Chichester, United Kingdom: John Wiley & Sons.
13
14     Grimm, A. G.; Fuhrer, J.  (1992) The response of spring wheat (Triticum aestivum L.) to ozone at higher
15            elevations: I. measurement of ozone and  carbon dioxide fluxes in open-top field chambers.  New Phytol.
16             121: 201-210.
17
18     Grosjean, D.;  Parmar, S. (1991) Removal of air  pollutant mixtures from museum display cases. Stud. Conserv.
19            36:  129-141.
20
21     Grosjean, D.;  Whitmore, P. M.;  De Moor, C. P.; Cass, G. R.; Druzik, J. R. (1987) Fading of alizarin and
22            relate artist's pigments by atmospheric ozone: reaction products and mechanisms. Environ. Sci. Technol.
23            21: 635-643.
24
25     Grosjean, D.;  Whitmore, P. M.;  Cass, G. R.; Druzik, J. R. (1988a) Ozone fading of natural organic colorants:
26            mechanisms and products of the reaction  of ozone with indigos. Environ. Sci. Technol. 22: 292-298.
27
28     Grosjean, D.;  Whitmore, P. M.;  De Moor, C. P.; Cass, G. R.; Druzik, J. R. (1988b) Ozone fading of organic
29            colorants: products and mechanism of the reaction of ozone with curcumin. Environ. Sci. Technol.
30            22:  1357-1361.
31
32     Grosjean, D.;  Whitmore, P. M.;  Cass, G. R.; Druzik, J. R. (1989) Ozone fading  of triphenylmethane colorants:
33            reaction products and mechanisms. Environ. Sci. Technol. 23: 1164-1167.
34
35     Grosjean, D.;  Grosjean, E.; Williams, E. L., II.  (1993) Fading of artists' colorants by a mixture of
36            photochemical oxidants. Atmos. Environ. Part A 27: 765-772.
37
38     Grulke, N. E.; Miller, P. R.; Wilborn, R. D.; Hahn, S. (1989) Photosynthetic response of giant sequoia
39            seedlings and rooted branchlets of mature foliage to ozone fumigation. In:  Olson, R. K.; Lefohn, A.  S.,
40            eds. Effects of air  pollution on western forests. Pittsburgh, PA: Air and Waste Management Association;
41            pp. 261-278 (Transactions series  no. 16).
42
43     Guderian, R.;  Tingey, D. T.; Rabe, R. (1985) Effects of photochemical oxidants on plants. In: Guderian, R.,
44            ed. Air pollution by photochemical oxidants:  formation, transport, control, and effects  on plants. Berlin,
45            Federal Republic of Germany: Springer-Verlag; pp. 127-333. (Billings, W. D.;  Golley, F.; Lange,
46            O. L.; Olson, J. S.; Remmert, H., eds. Ecological studies:  analysis and synthesis,  v. 52).
47
48     Gumpertz, M. L.;  Pantula, S. G. (1992) Nonlinear regression with variance components. J. Am. Stat. Assoc.
49            87: 201-209.
50
51     Gumpertz, M. G.;  Rawlings, J. O. (1991) Nonlinear regression for split-plot experiments. In: Proceedings of the
52             1990 Kansas State  University conference  on  applied statistics and agricultural experimental stations.
53            Manhattan, KS: pp. 156-168.
54


         December  1993                               5-371       DRAFT-DO NOT QUOTE OR CITE

-------
 1     Gurapertz, M. L.; Rawlings, J. O. (1992) Nonlinear regression with variance components: modeling effects of
 2            ozone on crop yield. Crop Sci. 32: 219-224.
 3
 4     Gupta, A. S.; Alscher, R. G.; MuCune, D. (1991) Response of photosynthesis and cellular antioxidants to ozone
 5            in Populus leaves. Plant Physiol. 96: 650-655.
 6
 7     Hagen, D. A.; Vincent, J. W.; Welle,  P. G. (1992) Benefits of preserving old-growth forests and the spotted
 8            owl. Contemp. Policy Issues 10: 13-26.
 9
10     Hain, F.  P. (1987) Interactions of insects, trees and air pollutants. Tree Physiol. 3: 93-102.
11
12     Hale-Marie, B.; Dutton, R.  G.; Allen, O. B.; Ormrod, D. P.; Goodyear, S. N.; Pyear, L. G. (1991) Design and
13            verification of a programmable gas dispensing system for exposing plants to dynamic concentrations of
14            air pollutants.  J.  Air Waste Manage. Assoc.  41: 460-463.
15
16     Hampp, R.; Einig, W.; Egger, B. (1990) Energy and redox status, and carbon allocation in one- to three-year-old
17            spruce needles. Environ. Pollut. 68: 305-318.
18
19     Hanley, N. D.; Ruffell, R. J. (1993) The contingent valuations of forest characteristics: tow experiments.
20            J. Agric. Econ. 44:  218-229.
21
22     Hanson,  G. P.; Addis, D. H. (1975) The stigma: not a selection site for ozone tolerance in Petunia hybrida.
23            Genetics 80: S40.
24
25     Hanson,  G. P.; Addis, D. H.; Thorne, L. (1976) Inheritance of photochemical air pollution tolerance in petunias.
26            Can.  J. Genet. Cytol. 18: 579-592.
27
28     Hanson,  P. J.; McLaughlin, S. B.; Edwards, N. T. (1988) Net CO2 exchange of Pinus taeda shoots exposed to
29            variable ozone levels and rain chemistries in field and laboratory settings. Physiol. Plant. 74: 635-642.
30
31     Harkov,  R.; Brennan, E. (1980) The influence of soil fertility and water stress on the ozone  response of hybrid
32            poplar trees. Phytopathology 70: 991-994.
33
34     Harkov,  R.; Brennan, E. (1982) The effect of acute ozone exposures on the growth of hybrid poplar. Plant Dis.
35            66: 587-589.
36
37     Harley, J.; Smith, S. (1983) Mycorrhizal symbiosis. New York, NY:  Academic Press; pp. 483.
38
39     Harwell, M.  A.; Cooper, W.; Flaak,  R. (1992) Prioritizing  ecological and human welfare risks from
40             environmental stresses. Environ.  Manage. 16: 451-464.
41
42     Hausladen, A.; Madamanchi, N.  R.; Fellows, S.; Alscher, R. G.; Amundson, R. G. (1990) Seasonal changes in
43             antioxidants in red spruce as affected by ozone. New Phytol. 115: 447-458.
44
45     Hayes, E. M.; Skelly, J. M. (1977) Transport of ozone from the northeast U.S. into Virginia and its effect on
46             eastern white  pines. Plant Dis. Rep. 61: 778-782.
47
48     Haylock, J. C.; Rush, J. L. (1976) Studies on the ozone fading of anthraquinone dyes on nylon fibers. Text. Res.
49             J. 46: 1-8.
50
51      Haylock, J. C.; Rush, J. L. (1978) Studies on the ozone fading of anthraquinone dyes on nylon fibers. Part II:
52             In-service performance. Text.  Res. J. 48: 143-149.
53
         December 1993                               5-372      DRAFT-DO NOT QUOTE OR CITE

-------
  1     Haynes, R. W.; Adams, D. M. (1992) Assessing economic impacts of air pollution damage to U.S. forests.
  2            In: deSteigner, J. E.,  ed. The economic impact of air pollution on timber markets. Washington, DC:
  3            U.S. Department of Agriculture, Southeastern Forest Experiment Station; general technical report no.
  4            SE-75.
  5
  6     Haynie, F. H.; Spence, J. W. (1984) Air pollution damage to exterior household paints. J. Air Pollut. Control
  7            Assoc. 34: 941-944.
  8
  9     Haynie, F. H.; Spence, J. W.; Upham, J. B. (1976) Effects of gaseous pollutants on materials—a chamber study.
 10            Research Triangle Park, NC: U.S.  Environmental Protection Agency, Environmental Sciences Research
 11            Laboratory; EPA report no. EPA-600/3-76/015. Available from: NTIS,  Springfield, VA; PB-251580.
 12
 13     Heagle, A. S. (1970) Effect of low-level ozone fumigations on crown rust of oats. Phytopathology 60: 252-254.
 14
 15     Heagle, A. S. (1975) Response of three obligate  parasites to ozone. Environ. Pollut. 9: 91-95.
 16
 17     Heagle, A. S. (1977) Effect of ozone on parasitism of corn by Helminthosporium maydis. Phytopathology
 18            67: 616-618.
 19
 20     Heagle, A. S. (1979a) Effects of growth media, fertiliser rate and hour and season of exposure on sensitivity of
 21            four soybean cultivars to ozone. Environ. Pollut. 18: 313-322.
 22
 23     Heagle, A. S. (1979b) Ranking of soybean cultivars for resistance to ozone using different ozone doses and
 24            response measures. Environ. Pollut. 19:  1-10.
 25
 26     Heagle, A. S.; Heck, W. W.  (1980) Field methods to assess crop losses due to oxidant air pollutants. In: Teng,
 27            P. S.; Krupa, S. V., eds. Crop loss assessment: proceedings of E. C. Stakman commemorative
 28            symposium. St. Paul,  MN: University of Minnesota, Agricultural Experiment Station; miscellaneous
 29            publication no. 7; pp. 296-305.
 30
 31     Heagle, A. S.; Key, L. W. (1973a) Effect of ozone on the wheat stem rust  fungus.  Phytopathology 63: 397-400.
 32
 33     Heagle, A. S.; Key, L. W. (1973b) Effect of Puccinia graminis f. sp. tritici on ozone injury hi wheat.
 34            Phytopathology 63: 609-613.
 35
 36     Heagle, A. S.; Letchworth, M. B. (1982) Relationships among injury, growth, and yield responses of soybean
 37            cultivars exposed to ozone at different light intensities. J. Environ. Qual. 11: 690-694.
 38
 39     Heagle, A. S.; Strickland, A.  (1972) Reaction of Erysiphe graminis f. sp. hordei to low levels of ozone.
 40            Phytopathology 62: 1144-1148.
 41
 42     Heagle, A. S.; Body, D. E.; Neely, G.  E. (1974) Injury and yield responses of soybean to chronic doses of
 43            ozone and sulfur dioxide in the field.  Phytopathology 64: 132-136.
 44
 45     Heagle, A. S.; Philbeck, R. B.; Letchworth, M.  B. (1979a) Injury and yield responses of spinach cultivars to
 46            chronic doses of ozone in open-top field chambers. J. Environ. Qual. 8:  368-373.
47
 48     Heagle, A. S.; Spencer, S.; Letchworth,  M. B. (1979b) Yield response of winter wheat to chronic doses of
49            ozone. Can. J. Bot. 57: 1999-2005.
50
51      Heagle, A. S.; Philbeck, R. B.; Rogers, H. H.; Letchworth, M.  B. (1979c) Dispensing and monitoring ozone in
52            open-top field chambers for plant-effects  studies. Phytopathology 69: 15-20.
53
         December 1993                               5.373       DRAFT-DO NOT QUOTE OR CITE

-------
  1      Heagle, A. S.; Letchworth, M. B.; Mitchell, C. A. (1983a) Effects of growth medium and fertilizer rate on the
  2             yield response of soybeans exposed to chronic doses of ozone. Phytopathology 73: 134-139.
  3
  4      Heagle, A. S.; Heck, W. W.; Rawlings, J. O.; Philbeck, R.  B. (1983b) Effects of chronic doses of ozone and
  5             sulfur dioxide on injury and yield of soybeans in open-top field chambers. Crop Sci. 23: 1184-1191.
  6
  7      Heagle, A. S.; Heck, W. W.; Lesser, V. M.; Rawlings, J. O.; Mowry, F. L. (1986a) Injury and yield response
  8             of cotton to chronic doses of ozone and sulfur dioxide. J. Environ. Qual. 15: 375-382.
  9
10      Heagle, A. S.; Lesser,  V. M.; Rawlings, J. O.; Heck, W. W.; Philbeck, R. B. (1986b) Response of soybeans to
11             chronic doses of ozone applied as constant or proportional additions to ambient air. Phytopathology
12             76: 51-56.
13
14      Heagle, A. S.; Flagler, R. B.; Patterson, R. P.; Lesser,  V. M.; Shafer, S. R.; Heck, W.  W. (1987a) Injury and
15             yield response of soybean to chronic doses of ozone and soil moisture deficit. Crop Sci.  27: 1016-1024.
16
17      Heagle, A. S.; Heck, W. W.; Lesser, V. M.; Rawlings, J. O. (1987b) Effects of daily ozone exposure duration
18             and concentration fluctuation on yield of tobacco. Phytopathology 77: 856-862.
19
20      Heagle, A. S.; Kress, L. W.; Temple, P. J.;  Kohut, R. J.; Miller, J. E.; Heggestad, H. E. (1988a) Factors
21             influencing ozone dose-yield response relationships in open-top field chamber studies. In: Heck,  W. W.;
22             Taylor, O. C.;  Tingey, eds. Assessment of crop loss from air pollutants. New York, NY: Elsevier
23             Applied Science; pp. 141-179.
24
25      Heagle, A. S.; Miller, J. E.; Heck, W. W.; Patterson, R. P. (1988b) Injury and yield response of cotton to
26             chronic doses of ozone and soil moisture deficit. J. Environ. Qual. 17: 627-635.
27
28      Heagle, A. S.; Rebbeck, J.; Shafer, S. R.; Blum, U.; Heck,  W. W. (1989) Effects of long-term ozone exposure
29             and soil moisture deficit on growth of a ladino clover-tall fescue pasture. Phytopathology 79: 128-136.
30
31      Heagle, A. S.; McLaughlin, M. R.;  Miller, J. E.; Joyner, R. L.; Spruill,  S. E. (1991a) Adaptation of a white
32             clover population to ozone stress. New  Phytol. 119: 61-68.
33
34      Heagle, A. S.; Miller, J. E.; Rawlings, J. O.; Vozzo, S. F. (1991b) Effect of growth stage on soybean response
35             to chronic  ozone exposure. J. Environ.  Qual. 20: 562-570.
36
37      Heagle, A. S.; McLaughlin, M. R.; Miller, J. E.; Joyner, R. L. (1992) Response of two white clover clones  to
38             peanut stunt virus and ozone.  Phytopathology 82: 254-258.
39
40      Heagle, A. S.; Miller, J. E.; Sherrill. D. E.; Rawlings,  J. O. (1993) Effects of ozone and carbon dioxide
41             mixtures on two clones of white clover. New Phytol. 123: 751-762.
42
43      Heath, R. L. (1987) Biochemical mechanisms of pollutant stress. In: Heck, W. W.;  Taylor, O. C.;  Tingey,
44             D. T., eds. Assessment of crop loss from air pollutants. New York, NY: Elsevier Applied Science;
45             pp. 259-286.
46
47      Heck, W. W. (1993) Ecological risk assessment case study: the National Crop Loss Assessment Network.
48             In: A review of ecological assessment case studies from a risk assessment perspective. Research Triangle
49             Park, NC: U.S. Environmental Protection Agency, Office of Health and Environmental Assessment,
50             Environmental  Criteria and Assessment Office; EPA  report no. EPA/630/R-92/005.
51
52      Heck, W. W.; Brandt,  C. S. (1977) Effects on vegetation: native, crops, forests. In: Stern, A. C., ed.  Air
53             pollution:  v. II. the effects of air pollution. 3rd. ed. New York, NY: Academic Press; pp. 157-229.
54


         December 1993                               5-374       DRAFT-DO NOT QUOTE OR CITE

-------
 1     Heck, W. W.; Heagle,  A.  S. (1970) Measurement of photochemical air pollution with a sensitive monitoring
 2            plant. J. Air Pollut. Control Assoc. 20: 97-99.
 3
 4     Heck, W. W.; Tingey,  D.  T. (1971) Ozone. Time-concentration model to predict acute foliar injury.
 5            In: Englund, H. M.; Beery, W. T., eds. Proceedings of the second international clean air congress;
 6            December 1970; Washington, DC. New York, NY:  Academic Press; pp. 249-255.
 7
 8     Heck, W. W.; Dunning, J. A,; Hindawi, I. J. (1965) Interactions of environmental factors on the sensitivity of
 9            plants to air pollution. J. Air Pollut. Control Assoc.  15: 511-515.
10
11     Heck, W. W.; Dunning, J. A.; Hindawi, I. J. (1966) Ozone: nonlinear relation of dose and injury in plants.
12            Science (Washington, DC) 151: 577-578.
13
14     Heck, W. W.; Fox, F.  L.; Brandt, C. S.; Dunning, J. A. (1969) Tobacco, a sensitive monitor for photochemical
15            air pollution.  Cincinnati, OH: U.S. Department of Health, Education, and Welfare, National Air
16            Pollution Control Administration; publication no. AP-55. Available from: NTTS, Springfield, VA;
17            PB-190257.
18
19     Heck, W. W.; Larsen,  R.  I.; Heagle, A. S.  (1980) Measuring the acute dose-response of plants to ozone.
20            In: Teng, P. S.; Rrupa, S. V., eds. Crop loss assessment: proceedings of E. C.  Stakman commemorative
21            symposium. St. Paul, MN: University of Minnesota, Agricultural Experiment Station; miscellaneous
22            publication no.  7; pp. 32-49.
23
24     Heck, W. W.; Taylor,  O.  C.; Adams, R.; Bingham, G.; Miller, J.; Preston, E.; Weinstein, L. (1982)
25            Assessment of crop loss from ozone. J. Air Pollut. Control Assoc. 32: 353-361.
26
27     Heck, W. W.; Adams,  R.  M.; Cure, W. W.; Heagle, A. S.; Heggestad, H.  E.; Kohut,  R. J.;  Kress, L. W.;
28            Rawlings, J. O.; Taylor, O.  C. (1983) A reassessment of crop loss from ozone.  Environ. Sci. Technol.
29             17: 573A-581A.
30
31     Heck, W. W.; Cure,  W. W.; Rawlings, J. O.; Zaragoza, L. J.; Heagle, A. S.; Heggestad, H. E.; Kohut, R. J.;
32            Kress, L. W.; Temple, P. J. (1984) Assessing impacts of ozone on agricultural crops: n. crop yield
33            functions and alternative exposure statistics.  J. Air Pollut. Control Assoc. 34: 810-817.
34
35     Heck, W. W.; Dunning, J. A.; Reinert, R. A.; Prior, S. A.; Rangappa, M.; Benepal, P. S. (1988) Differential
36            responses of four bean cultivars to chronic doses of  ozone. J. Am. Soc.  Hortic.  Sci. 113: 46-51.
37
38     Heck, W. W.; Heagle,  A.  S.; Miller, J. E.; Rawlings, J. O. (1991) A national program (NCLAN) to assess the
39            impact of ozone on agricultural resources. In: Berglund, R.  L.; Lawson, D. R.; McKee, D. J.,  eds.
40            Tropospheric ozone and the environment: papers from an international conference; March 1990;
41            Los Angeles, CA.  Pittsburgh, PA: Air & Waste Management Association; pp. 225-254. (A&WMA
42            transaction series no. TR-19).
43
44     Heggestad, H. E. (1988) Reduction in soybean seed yields by ozone air pollution? JAPCA 38:  1040-1041.
45
46     Heggestad, H. E.;  Bennett, J. H. (1981) Photochemical oxidants potentiate yield losses in snap beans attributable
47            to sulfur dioxide. Science (Washington, DC) 213: 1008-1010.
48
49     Heggestad, H. E.;  Lesser,  V. M. (1990) Effects of ozone, sulfur dioxide, soil water deficit, and cultivar on
50            yields of soybean.  J. Environ. Qual. 19: 488-495.
51
52     Heggestad, H. E.;  Middleton, J. T. (1959) Ozone in high concentrations as cause of tobacco leaf injury. Science
53            (Washington, DC)  129: 208-210.
54


         December 1993                               5.375       DRAFT-DO NOT QUOTE OR CITE

-------
 1     Henderson, W. R.; Reinert, R. A. (1979) Yield response of four fresh market tomato cultivars after acute ozone
 2            exposure in the seedling stage. J. Am. Soc. Hortic. Sci. 104: 754-759.
 3
 4     Heggestad, H. E.; Gish, T. J.; Lee, E. H.; Douglass, W. L. (1984) The effects of Oj and soil moisture stress on
 5            productivity of two soybean cultivars, 1983. In: Heck,  W. W.; Taylor, O. C.; Adams, R. M.; Miller,
 6            J. E.; Preston, E. M.; Weinstein, L. H., eds. National crop loss assessment network (NCLAN) 1983
 7            annual report.  Corvallis, OR: U.S. Environmental Protection Agency, Corvallis Environmental Research
 8            Laboratory; pp. 74-102; EPA report no. EPA 600/3-85-061. Available from: NTIS, Springfield, VA;
 9            PB85-236859/HSU.
10
11     Heggestad, H. E.; Gish, T. J.; Lee, E. H.; Bennett, J. H.; Douglass, L. W.  (1985) Interaction of soil moisture
12            stress and ambient ozone on growth and yields of soybeans. Phytopathology 75: 472-477.
13
14     Heggestad, H. E.; Anderson, E. L.; Gish, T. J.;  Lee, E. H. (1988) Effects of ozone and soil water deficit on
15            roots and shoots of field-grown soybeans. Environ. Pollut.  50: 259-278.
16
17     Hernandez-Tejeda, T.; de Bauer, L. I. (1984) Evolucion del dano por gases oxidantes  en Pinus hartwegii y Plnus
18            montezumae var. Lindleyi en el Ajusco, D.F. Agrociencia 56:  183-194.
19
20     Hershaft, A.; Freeman, A. M., Ill; Crocker, T. D.; Stevens, J. B. (1978) Critical review of estimating benefits
21            of air and water pollution control.  Washington, DC: U.S. Environmental Protection Agency, Office of
22            Research and Development; EPA report no. EPA-600/5-78-014. Available from: NTIS, Springfield, VA;
23            PB-285555.
24
25     Hibben,  C. R.; Taylor, M.  P. (1975) Ozone and sulphur dioxide effects on the lilac powdery mildew  fungus.
26            Environ. Pollut. 9:  107-114.
27
28     Hicks, B. B.; Baldocchi, D. D.; Meyers, T. P.; Hosker, R. P., Jr.; Matt, D. R. (1987) A preliminary multiple
29            resistance routine for deriving dry deposition velocities from measured quantities. Water Air Soil Pollut.
30            36: 311-330.
31
32     Higgs, E. S. (1987) Changing value perspectives in natural resource allocation. Trans. Am. Fish. Soc.
33             116: 525-531.
34
35     Hiltbrunner, E.;  Fluckiger, W. (1992) Altered feeding preference of beech weevil (Khynchaenus fagi  L. for
36            beech foliage under ambient air pollution. Environ. Pollut. 75:  333-336.
37
38     Hinckley, T.; Ford, D.; Segura, G.; Spnigel, D. (1992) Key processes from tree to stand level. In: Wall, G.,
39            ed. Implications of climate change for Pacific Northwest forest management.  Waterloo, Ontario, Canada:
40            University of Waterloo, Department of Geography; pp. 33-43.  (Department of Geography publication
41             series, occasional paper no. 15).
42
43     Hofmann, C. M.; Miller, R. L. (1969) Resistance of passenger tires to atmospheric exposure. J. Mater.
44            4: 31-43.
45
46    Hofstra, G.; Beckerson, D. W. (1981) Foliar responses of five plant species  to ozone and a sulphur
47            dioxide/ozone mixture after a sulphur dioxide pre-exposure. Atmos. Environ.  15: 383-389.
48
49     Hofstra, G.; Tonneijck, A. E. G.; Allen,  O.  B. (1985) Cumulative effects of low levels of SO2 on O3 sensitivity
50            in bean and cucumber. Atmos. Environ.  19: 195-198.
51
52     Hogsett, W. E.; Tingey, D. T. (1990) A comparison of remote and rural ozone exposure regimes on trees.
53            Presented at: the International Congress of Ecology; August; Yokohama, Japan.
54


         December 1993                              5-376       DRAFT-DO NOT QUOTE OR CITE

-------
  1      Hogsett, W. E.; Plocher, M.; Wildman, V.; Tingey, D. T.; Bennett, J. P. (1985a) Growth response of two
  2             varieties of slash pine seedlings to chronic ozone exposures. Can. J. Bot. 63: 2369-2376.
  3
  4      Hogsett, W. E.; Tingey, D. T.; Holman, S. R. (1985b) A programmable exposure control system for
  5             determination of the effects of pollutant exposure regimes on plant growth. Atmos. Environ.
  6             19: 1135-1145.
  7
  8      Hogsett, W. E.; Olszyk, D.; Ormrod, D. P.; Taylor, G. E., Jr.; Tingey, D. T. (1987a) Air pollution exposure
  9             systems and experimental protocols. Volume I:  a review and evaluation of performance. Corvallis, OR:
10             U.S. Environmental Protection Agency, Corvallis Environmental Research Laboratory; EPA report
11             no. EPA 600/3-87/037a. Available from: NTIS, Springfield, VA; PB88-181680/HSU.
12
13      Hogsett, W. E.; Olszyk, D. M.; Ormrod, D. P.; Taylor, G. E., Jr.; Tingey, D.  T. (1987b) Air pollution
14             exposure systems and experimental protocols: volume 2: description of facilities. Corvallis, OR: U.S.
15             Environmental Protection Agency, Corvallis Environmental Research laboratory;  EPA report no.
16             EPA/600/3-87/037b. Available from: NTIS, Springfield, VA; PB88-181698.
17
18      Hogsett, W. E.; Tingey, D. T.; Lee, E. H. (1988) Ozone exposure indices: concepts for development and
19             evaluation of their use. In: Heck, W. W.; Taylor, O. C.; Tingey, D. T., eds. Assessment of crop  loss
20             from air pollutants: proceedings of an international conference;  October 1987; Raleigh, NC. New York,
21             NY: Elsevier Applied Science; pp.  107-138.
22
23      Hogsett, W. E.; Tingey, D. T.; Hendricks, C.; Rossi,  D. (1989) Sensitivity of western conifers to SOj and
24             seasonal interaction of acid fog and ozone. In: Olson, R. K.; Lefohn, A.  S., eds. Transactions: effects of
25             air pollution on western forests; June; Anaheim, CA. Pittsburgh, PA: Air Pollution Control Associations;
26             pp. 469-491.
27
28      Hogsett, W. E.; Herstrom, A.; Laurence, J. A.; Weber, J.; Lee,  E. H.; Tingey, D. T. (1993) Ecosystem
29             exposure assessment: ozone risks to forests.  In: Comparative risk analysis and priority setting of air
30             pollution issues. Pittsburgh, PA: Air and Waste Management Association: hi press.
31
32      Holley, J. D.; Hofstra, G.; Hall, R. (1985) Effect of reducing oxidant injury and early blight on fresh weight and
33             tuber density of potato. Phytopathology 75: 529-532.
34
35      Horton, S. J.; Reinert, R.  A.; Heck,  W. W. (1990) Effects of ozone on three open-pollinated families of Pinus
36             taeda L. grown  in two substrates. Environ. Pollut. 65: 279-292.
37
38      Hosker, R. P., Jr.; Lindberg, S. E. (1982) Review:  atmospheric deposition and plant assimilation of gases and
39             particles.  Atmos. Environ. 16: 889-910.
40
41      Houpis, J. L.; Costella,  M. P.; Cowles, S. (1991) A branch exposure chamber for fumigating ponderosa pine to
42             atmospheric pollution. J. Environ. Qual. 20: 467-474.
43
44      Houston, D. B. (1974) Response of selected Pinus strobus L. clones to fumigations with sulfur dioxide and
45             ozone.  Can. J. For. Res. 4: 65-68.
46
47      Houston, D. B.; Dochinger, L. S. (1977) Effects of ambient air pollution on cone, seed, and pollen
48             characteristics in eastern white and  red pines. Environ. Pollut. 12:  1-5.
49
50      Houston, D. B.; Stairs, G. R. (1973) Genetic control of sulfur dioxide and ozone tolerance in eastern white pine.
51             For. Sci.  19: 267-271.
52
53      Howarth, R. B.; Norgaard, R. B. (1992) Environmental valuation under sustainable development. Am. Econ.
54             Rev. 82: 473-477.


         December 1993                               5.377       DRAFT-DO NOT QUOTE OR CITE

-------
 1     Howell, R. K.; Graham, J. H. (1977) Interaction of ozone and bacterial leafspot of alfalfa. Plant Dis. Rep.
 2            61: 565-567.
 3
 4     Huang, T. R.; Aycock, M. K., Jr.; Mulchi, C. L. (1975) Heterosis and combining ability estimates for air
 5            pollution damage, primarily ozone, in Maryland tobacco. Crop Sci.  15: 785-789.
 6
 7     Hucl, P.; Beversdorf, W. D. (1982a) The response of selected Phaseolus vulgaris L. cultivars to ozone under
 8            controlled fumigation and ambient field levels. Can. J. Plant Sci. 62: 561-569.
 9
10     Hucl, P.; Beversdorf, W. D. (1982b) The inheritance of ozone insensitivity in selected Phaseolus vulgaris L.
11            populations. Can. J. Plant Sci. 62: 861-865.
12
13     Huevel, H. M.; Huisman,  R.; Schmidt, H. M. (1978) Ozone fading of disperse blue 3  on nylon 6 fibers. The
14            influence of physical fiber properties. Text. Res. J. 48: 376-384.
15
16     Hughes, P. R. (1988) Insect populations on host plants subjected to air pollution. In: Heinricks, E.  A.,
17            ed. Plant-stress-insect  interactions. New York, NY: Wiley and  Sons; pp. 249-319.
18
19     Hyde, W. F. (1989) Marginal costs of managing endangered species: the case of the red-cockheaded woodpecker.
20            J. Agric. Econ. Res. 41: 12-19.
21
22     Ingham, R. E.; Trofymow, J.  A.; Ingham, E. R.; Coleman, D. C. (1985) Interactions of bacteria,  fungi and
23            their nematode grazers: effects on nutrient cycling and plant growth. Ecol. Monogr. 55: 119-140.
24
25     Irving, P. M.; Kress, L. W.;  Prepejchal, W.; Smith, H. J. (1988) Studies on the interaction of ozone with
26            drought stress or with sulfur dioxide on soybeans and corn.  Argonne, IL: U.S. Environmental Protection
27            Agency; Argonne National Laboratory; technical report no.  ANL-88-31.
28
29     Jacobson, J. S. (1977) The effects of photochemical oxidants on vegetation. In: Ozon und Begleitsubstanzen
30            im photochemischen Smog:  das Kolloquium [Ozone and related substances in photochemical smog: the
31            colloquium]; September 1976; Dusseldorf, Federal Republic of Germany. Dusseldorf, Federal Republic
32            of Germany: VDI-Verlag GmbH; pp. 163-173. (VDI-Berichte nr. 270).
33
34     James, R. L.; Cobb, F. W., Jr.; Miller, P. R.; Parmeter, J. R.,  Jr. (1980)  Effects of oxidant air pollution on
35            susceptibility of pine roots to Fames annosus. Phytopathology 70: 560-563.
36
37     Jarvis, P. G.; McNaughton, K. G. (1986) Stomatal control of transpiration. Adv. Ecol. Res. 15: 1-49.
38
39     Jeffords, M. R.; Endress, A. G. (1984) Possible role of ozone in tree defoliation by the gypsy moth
40            (Lepidoptera: Lymantriidae). Environ. Entomol. 13: 1249-1252.
41
42     Jensen, K. F.  (1981a) Ozone fumigation decreased the root carbohydrate content and dry weight of green ash
43            seedlings. Environ. Pollut. Ser. A 26: 147-152.
44
45     Jensen, K. F.  (1981b) Growth analysis of hybrid poplar cuttings  fumigated with ozone  and sulphur dioxide.
46            Environ. Pollut. Ser. A 26: 243-250.
47
48     Jensen, K. F.; Dochinger, L.  S. (1989) Response of eastern hardwood species to ozone, sulfur dioxide and acid
49            precipitation. JAPCA  39: 852-855.
50
51     Jensen, K. F.; Patton, R. L. (1990) Response of yellow-poplar Liriodendron tulipifera L. seedlings to simulated
52            acid ram and ozone I. growth modifications. Environ. Exp. Bot. 30: 59-66.
53
         December 1993                              5-378       DRAFT-DO NOT QUOTE OR CITE

-------
 1     Jensen, K. F.; Roberts, B. R. (1986) Changes in yellow poplar stomatal resistance with SO2 and O3 fumigation.
 2            Environ. Pollut. Ser. A 41: 235-245.
 3
 4     Johnsen,  I.;  Mortensen, L.; Moseholm,  L.; Ro-Poulsen, H. (1992) Ozone sensitivity of open-top chamber grown
 5            cultivars of spring wheat and spring rape. Air Pollut.  Ecosyst. (): 637-640.
 6
 7     Johnson, N.; Adams, R. M. (1989) On the marginal value of a fish: some evidence from a steelhead fishery.
 8            Mar. Resour. Econ. 6: 43-55.
 9
10     Johnson, D. W.; Taylor,  G. E. (1989) Role of air pollution in forest decline in eastern North America. Water
11            Air Soil Pollut. 48: 21-43.
12
13     Johnston, J.  W., Jr.; Shriner, D. S. (1986) Yield response of Davis soybeans to simulated acid rain and gaseous
14            pollutants in the field. New Phytol. 103: 695-708.
15
16     Johnston, W. J.; Haaland, R.  L.; Dickens, R. (1983) Inheritance of ozone resistance in tall fescue. Crop Sci.
17            23: 235-236.
18
19     Jones, P. D. (1989) Global temperature  variations since 1861: the influence of the southern oscillation and a look
20            at recent trends. In: Crutzen, J.  C.; Gerard, P. J.; Zander, R., eds. Proceedings of the 28th international
21            astrophysical colloqium. Universite de Liege; pp. 287-302.
22
23     Jones, H. G. (1992) Plant and microclimate: a quantitative approach to environmental plant physiology. 2nd ed.
24            Cambridge,  United Kingdom: Cambridge University Press; pp. 32-41.
25
26     Jones, C. G.; Coleman, J. S.  (1988) Plant stress and insect behavior: cottonwood, ozone and the feeding and
27            oviposition preference of a beetle. Oecologia 76: 51-56.
28
29     Jones, H. C.; Noggle, J.  C.; McDuffie, C., Jr. (1988) Effects of chronic exposure to simulated power plant
30            emissions and ozone on soybean production. J. Environ. Qual.  17: 701-707.
31
32     Kamath,  Y.  K.; Ruetsch,  S. B.; Weigmann, H.-D. (1983) Microspectrophotometric study of ozone fading of
33            disperse dyes in nylon. Text. Res. J. 53: 391-402.
34
35     Kargiolaki, H.; Osborne,  D. J.; Thompson, F. B. (1991)  Leaf abscission and stem lesions (intumescences) on
36            poplar clones after SO2 and O3  fumigation: a link with ethylene release? J. Exp. Bot. 42: 1189-1198.
37
38     Karnosky, D. F. (1977) Evidence  for genetic control of response to sulfur dioxide and ozone in Populus
39            tremuloides. Can. J.  For. Res. 7:  437-440.
40
41     Karnosky, D. F. (198la)  Chamber and field evaluations of air pollution tolerances of urban trees. J. Arboric.
42            7: 99-105.
43
44     Karnosky, D. F. (198 Ib) Changes in eastern white pine stands related to ozone stress. Mitt. Forstl.
45            Bundesversuchsanst.  Wien 137:  41-45.
46
47     Karnosky, D. F. (1989a)  Mechanisms of genetic control of air pollution tolerance  in forest trees. In: Noble,
48            R. D.;  Martin, J. L.;  Jensen, K. F., eds. Proceedings of the 2nd US-USSR symposium on air pollution
49            effects on vegetation.  Broomall, PA: USDA Forest Service Northeastern Forest Experiment Station;
50            pp.  127-134.
51
52     Karnosky, D. F. (1989b) Air-pollution induced population changes in North American forests. In: Bucher, J. B.;
53            Bucher-Wallin, I., eds. Air pollution and forest decline; v. I; pp. 315-317.
54


         December 1993                               5-379       DRAFT-DO NOT QUOTE OR CITE

-------
  1      Karnosky, D. F. (1991) Ecological genetics and changes in atmospheric chemistry: the application of knowledge.
  2             In: Taylor, G. E., Jr.; Pitelka, L. F.; Clegg, M. T., eds. Ecological genetics and air pollution. New
  3             York, NY: Springer-Verlag; pp. 321-336.
  4
  5      Karnosky, D. F.; Steiner, K.  C. (1981) Provenance and family variation in response of Fraxinum americana and
  6             F. pennsylvanica to ozone and sulfur dioxide. Phytopathology 71: 804-807.
  7
  8      Karnosky, D. F.; Scholz, F.;  Geburek, T.; Rudin, D. (1989) Implications of genetic effects of air pollution on
  9             forest ecosystems—knowledge gaps. In: Scholz, F.; Gregorius,  H.-R.; Rudin, D., eds. Genetic effects of
10             air pollutants in  forest tree populations: proceedings of the joint meeting of the IUFRO working parties;
11             August 1987; Grosshansdorf, West Germany. Berlin, Germany: Springer-Verlag; pp. 199-201.
12
13      Karnosky, D. F.; Gagnon, Z. E.; Reed, D. D.; Witter, J. A. (1992a) Effects of genotype on the response of
14             Populus tremuloldes Michx. to ozone and nitrogen deposition. Water Air Soil Pollut. 62: 189-199.

16      Karnosky, D. F.; Gagnon, Z. E.; Reed, D. D.; Witter, J. A. (1992b) Growth and biomass allocation of
17             symptomatic and asymptomatic Populus tremuloides clones in response to seasonal ozone exposures.  Can.
18             J. For. Res. 22: 1785-1788.
19
20      Karnosky, D. F.; Dickson, R. E.; Gagnon, Z. E.; Coleman, E. D.; Lee, H.; Isebrands, J. G. (1993) Changes in
21             growth, leaf abscission and biomass associated with seasonal ozone exposures of Populus tremuloides
22             clones and seedlings. Submitted.
23
24      Karr, J. (1987) Biological monitoring and environmental assessment:  a  conceptual framework. Environ. Manage.
25             11:249-256.
26
27      Kasana, M. S.  (1991) Sensitivity of three leguminous crops to ozone  as influenced by different stages of growth
28             and development. Environ.  Pollut. 69:  131-149.
29
30      Kasana, M. S.  (1992) Effects  of ozone fumigation on a tropical fibre plant, kenaf (Hibiscus cannabinus L.).
31             Agric. Ecosyst. Environ. 38: 61-70.
32
33      Kats, G.;  Dawson, P. J.; Bytnerowicz, A.; Wolf, J. W.; Thompson, C. R.; Olszyk, D. M.  (1985) Effects of
34             ozone or sulfur dioxide on growth and  yield of rice. Agric. Ecosyst. Environ. 14: 103-117.
35
36      Keane, K. D.;  Manning, W. J. (1988) Effects of ozone and simulated acid rain on birch seedling growth and
37             formation of ectomycorrhizae. Environ. Pollut. 52: 55-66.
38
39      Keeling, C. D. et al. (1989) A three-dimensional model of atmospheric CO2 transport based on observed winds:
40             1. analysis of observational data. In: Peterson, D. H., ed. Aspects of climate variability in the Pacific
41             and the western  Americas. Washington, DC: American Geophysical Union; pp. 165-236 (Geophysical
42             monograph no. 55).
43
44      Kelleher,  T. J.; Feder, W. A. (1978) Phytotoxic concentrations of ozone on Nantucket Island: long range
45             transport from the middle Atlantic states over the open ocean confirmed by bioassay with ozone-sensitive
46             tobacco plants. Environ. Pollut. 17: 187-194.
47
48      Keller, T. (1988) Growth and premature leaf fall in American aspen as  bioindications for ozone. Environ. Pollut.
49             52: 183-192.
50
51      Keller (1989).
52
53      Keller, T.; Matyssek, R. (1990) Limited compensation of ozone stress by potassium in Norway spruce. Environ.
54             Pollut. 67: 1-14.


         December 1993                               5-380       DRAFT-DO NOT QUOTE  OR CITE

-------
  1      Kendrick, J.  B., Jr.; Middleton, J. T.; Darley, E. F. (1954) Chemical protection of plants from ozonated olefin
  2             (smog) injury. Phytopathology 44: 494-495.
  3
  4      Kerfourn, C.; Garrec, J. P. (1992) Modifications in the alkane composition of cuticular waxes from spruce
  5             needles (Picea abies) and ivy leaves (Hedera helix) exposed to ozone fumigation and acid fog:
  6             comparison with needles from declining spruce trees. Can. J. Bot. 70: 861-869.
  7
  8      Kerr, N.; Morris, M. A.; Zeronian, S. H. (1969) The effect of ozone and laundering on a vat-dyed cotton fabric.
  9             Am.  Dyest. Rep. 58: 34-36.
10
11      Kerstiens, G.; Lendzian, K. J.  (1989) Interaction between ozone and plant cuticles: I. ozone deposition and
12             permeability. New Phytol. 112: 13-19.
13
14      Kickert, R. N.; Krupa, S. V. (1991) Modeling plant response  to tropospheric ozone: a critical review. Environ.
15             Pollut. 70: 271-383.
16
17      King, D. A.  (1987) A model for predicting the influence of moisture stress on crop losses caused by ozone. Ecol.
18             Modelling 35: 29-44.
19
20      Knudson-Butler, L.  K.; Tibbitts, T. W. (1979) Variation in ozone sensitivity and symptom expression among
21             cultivars of Phaseolus vulgaris L. J. Amer.  Soc. Hort. Sci. 104: 208-210.
22
23      Kobayashi, K.; Miller, J. E.; Flagler, R. B.; Heck, W. W. (1990) Modeling the effects of ozone on soybean
24             growth and  yield. Environ. Pollut. 65: 33-64.
25
26      Kohut,  R. J.; Amundson, R. G.; Laurence, J. A. (1986) Evaluation of growth and yield of soybean exposed to
27             ozone in the field. Environ. Pollut. Ser.  A 41: 219-234.
28
29      Kohut,  R. J.; Amundson, R. G.; Laurence, J. A.; Colavito, L.;  Van Leuken, P.; King, P. (1987) Effects of
30             ozone and sulfur dioxide on yield of winter wheat. Phytopathology 77: 71-74.
31
32      Kohut,  R. J.; Laurence, J. A.; Amundson, R. G. (1988a) Effects of ozone and sulfur dioxide on yield of red
33             clover and timothy. J. Environ. Qual. 17: 580-585.
34
35      Kohut,  R. J.; Laurence, J. A.; Colavito, L. J. (1988b) The influence of ozone exposure dynamics on the growth
36             and yield of kidney bean. Environ. Pollut. 53: 79-88.
37
38      Kohut,  R. J.; Laurence, J. A.; Amundson, R. G.; Raba, R. M.; Melkonian, J. J. (1990) Effects of ozone and
39             acidic precipitation on the growth and photosynthesis of red spruce after two years of exposure. Water
40             Air Soil Pollut. 51: 277-286.
41
42      Kopp, R. J. (1992)  Why existence values should be used in cost-benefit analysis. J. Policy Anal. Manage.
43             11: 123-130.
44
45      Kopp, R. J.;  Krupnick, A. J. (1987) Agricultural policy and the  benefits of ozone control. Am. J. Agric. Econ.
46             69: 956-962.
47
48      Kopp, R.; Vaughn,  W.; Hazilla, M.;  Carson, R. (1985) Implications of environmental policy for U.S.
49             agriculture:  the case of ambient ozone standards. J. Environ. Econ. Manage. 20: 321-331.
50
51      Kostka-Rick,  R.; Manning, W. J. (1992a) Partitioning of biomass and carbohydrates hi field-grown radish under
52             ambient concentrations  of ozone, and treated with the anti-ozonant ethylene-diurea (EDU). New Phytol.
53             121:  187-200.
54


         December 1993                               5-381       DRAFT-DO NOT QUOTE OR CITE

-------
 1     Kostka-Rick, R.; Manning, W. J. (1992b) Effects and interactions of ozone and the anti-ozonant EDU at different
 2             stages of radish Raphanus sativus. 1. Development. J. Exp. Bot. 43: 1621-1631.
 3
 4     Kostka-Rick, R.; Manning, W. J. (1993) Dose-response studies with ethylenediurea (EDU) and radish. Environ.
 5             Pollut. 79: 249-260.
 6
 7     Kramer, G. F.; Lee, E. H.; Rowland, R. A.; Mulchi, C. L. (1991) Effects of elevated CO2 concentration on the
 8             polyamine levels of field-grown soybean at three 03 regimes. Environ. Pollut. 73: 137-152.
 9
10     Kramer; Kozlowski; Pallardy. (1992)
11
12     Krause, C. R.; Weidensaul, T. C. (1978) Effects of ozone on the sporulation, germination, and pathogenicity of
13             Botrytis cinerea. Phytopathology 68: 195-198.
14
15     Krause, G. H. M.; Riley,  W. D.; Feder, W. A. (1975) Effects of ozone on petunia and tomato pollen tube
16             elongation in vivo. Proc. Am.  Phytopathol. Soc. 2:  100.
17
18     Kress, L. W.; Skelly, J. M. (1982) Response of several eastern forest tree species to chronic doses of ozone and
19             nitrogen dioxide. Plant Dis. 66: 1149-1152.
20
21     Kress, L. W.; Skelly, J. M.; Hinkelmann, K. H. (1982a) Relative sensitivity of 18 full-sib families of Pinus
22             taeda to O3. Can.  J. For. Res. 12: 203-209.
23
24     Kress, L. W.; Skelly, J. M.; Hinkelmann, K. H. (1982b) Growth impact of O3, NO2 and/or SO2 on Pinus
25             taeda. Environ. Monit.  Assess. 1: 229-239.
26
27     Kress, L. W.; Miller, J. E.; Smith, H. J.; Rawlings, J. O. (1986) Impact of ozone and sulphur dioxide on
28             soybean yield. Environ. Pollut. Ser. A 41: 105-123.
29
30     Kress, L. W.; Allen, H. L.; Mudons, J. E.; Heck, W. W. (1988) Response of loblolly pine to acidic
31             precipitation and ozone. Presented at: 81st annual meeting of the Air Pollution Control Association; June;
32             Dallas, TX. Pittsburgh, PA: Air Pollution Control Association;  paper no. 88-705.
33
34     Kress, L. W.; Allen, H. L.; Mudano, J. E.; Stow, T. K. (1992) Impact of ozone on loblolly pine seedling
35             foliage production and retention. Environ. Toxicol. Chem. 11: 1115-1128.
36
37     Krupa, S.; Kickert, R. N. (1987) An analysis of numerical models of air pollutant exposure and vegetation
38             response. Environ. Pollut. 44: 127-158.
39
40     Krupa, S. V.; Kickert, R. N. (1989) The greenhouse effect: impacts of ultraviolet-B (UV-B) radiation, carbon
41             dioxide (CC>2), and ozone (O3) on vegetation. Environ. Pollut. 61: 263-393.
42
43     Krupa, S. V.; Nosal, M. (1989) Effects of ozone on agricultural crops.  In: Schneider, T.; Lee, S. D.; Wolters,
44             G. J. R.; Grant, L. D., eds. Atmospheric ozone research and its policy implications: proceedings  of the
45             3rd US-Dutch international symposium; May 1988; Nijmegen, The Netherlands. Amsterdam, The
46            Netherlands: Elsevier Science  Publishers; pp. 229-238. (Studies hi environmental science 35).
47
48     Krupa, S. V.; Teng, P. S. (1982) Uncertainties in estimating ecological effects of air pollutants. In: Proceedings
49            of the 75th annual meeting of the Air Pollution Control  Association; June; New Orleans, LA. Pittsburgh,
50            PA: Air Pollution Control Association; 82-6.1.
51
52     Kuikman, P. J.; Van Elsas, J. D.; Jassen, A. G.; Burgers, S. L. G. E.; Van Veen, J. A. (1990) Population
53            dynamics  and activity of bacteria and protozoa in relation to their spatial distribution in soil. Soil Biol.
54            Biochem.  22: 1063-1073.


          December 1993                               5-382       DRAFT-DO  NOT QUOTE OR CITE

-------
  1      Lackner, A. L.; Alexander, S. A. (1983) Root disease and insect infestations on air-pollution-sensitive Pinus
  2             strobus and studies of pathogenicity of Verticidadiella procera. Plant Dis. 67: 679-681.
  3
  4      Laisk, A.; Kull, O.; Moldau, H. (1989) Ozone concentration in leaf intercellular air spaces is close to zero. Plant
  5             Physiol. 90: 1163-1167.
  6
  7      Lake, G. J.; Mente, P. G. (1992) Ozone cracking and protection of elastomers at high and low temperatures.
  8             J. Nat. Rubber Res. 7: 1-13.
  9
10      Langebartels,  C.; Kerner, K.; Leonardi, S.; Schraudner, M.; Trost, M.; Heller, W.; Sandermann, H., Jr.  (1991)
11             Biochemical plant responses to ozone: I. differential  induction of polyamine and ethylene biosynthesis in
12             tobacco. Plant Physiol. 95: 882-889.
13
14      Larsen, R. I.; Heck, W.  W. (1984) An air quality data analysis system for interrelating  effects, standards,  and
15             needed source reductions: part 8. an effective mean O3 crop reduction mathematical model. J. Air Pollut.
16             Control. Assoc. 34: 1023-1034.
17
18      Larsen, R. I.; Heagle, A. S.; Heck, W.  W. (1983) An air quality data analysis system for interrelating effects,
19             standards, and needed source reductions: part 7. an 03-802 leaf injury mathematical model. J. Air
20             Pollut. Control Assoc. 33:  198-207.
21
22      Larsen, R. I.; McCurdy, T. R.; Johnson, P. M.; Heck, W.  W. (1988) An air quality data analysis system for
23             interrelating effects, standards, and needed source reductions: part 10. potential  ambient O3 standards to
24             limit soybean crop reduction. JAPCA 38: 1497-1503.
25
26      Larsen, J.  B.; Yang, W.; Tiedemann, A. V. (1990) Effects of ozone on gas exchange, frost resistance, flushing
27             and growth of different provenances of European silver fir (Abies alba Mill.). Eur. J. For. Pathol.
28             20:211-218.
29
30      Lattimer, R. P.; Layer, R. W.; Rhee, C. K. (1984) Mechanisms of antiozonant protection: antiozonant-rubber
31             reactions during ozone exposure.  In: 32nd annual conference on mass spectrometry and allied topics.
32             Bethesda, MD: American Society for Mass Spectrometry; pp. 357-358.
33
34      Laurence,  J. A.; Wood, F. A. (1978a) Effects of ozone on infection of soybean by Pseudomonas glycinea.
35             Phytopathology 68: 441-445.
36
37      I^aurence,  J. A.; Wood, F. A. (1978b) Effect of ozone on infection of wild strawberry by Xanthomonas
38             fragariae. Phytopathology 68: 689-692.
39
40      Laurence, J. A.; Kohut, R. J.; Amundson, R. G. (1989) Response of red spruce seedlings exposed to ozone and
41             simulated acidic precipitation in the field. Arch. Environ. Contam. Toxicol. 18:  285-290.
42
43      Laurence, J. A.; Kohut, R. J.; Amundson, R. G. (1993a) Use of TREGRO to simulate  the effects of ozone on
44             the growth of red spruce seedlings. For. Sci.: in press.
45
46      Laurence, J. A.; Amundson, R. G.; Friend, A. L.; Pell, E.  J.; Temple, P. J.  (1993b) Allocation of carbon in
47             plants under stress: an analysis of the ROPIS experiments. J.  Environ. Qual.: in press.
48
49      Le Sueur-Brymer, N. M.; Ormrod, D. P. (1984) Carbon dioxide exchange rates of fruiting soybean plants
50             exposed to ozone and sulphur dioxide singly or in combination. Can. J. Plant Sci. 64: 69-75.
51
52      Lechowicz, M. J. (1987) Resource allocation by plants under air pollution stress: implications for
53             plant-pest-pathogen interactions. Bot. Rev. 53: 281-300.
54


         December  1993                               5-383       DRAFT-DO NOT  QUOTE OR CITE

-------
 1     Lee, E. H.; Bennett, J. H. (1982) Superoxide dismutase: a possible protective enzyme against ozone injury in
 2             snap beans (Phaseolus vulgaris L.). Plant Physiol. 69: 1444-1449.
 3
 4     Lee, J. J.;  Preston, E. M.; Lewis, R. A. (1978) A system for the experimental evaluation of the ecological
 5             effects of sulfur dioxide. In: Proceedings of the 4th joint conference on sensing of environmental
 6             pollutants; November 1977; New Orleans, LA.  Washington, DC: American Chemical Society; pp. 49-53.
 7
 8     Lee, E. H.; Tingey, D. T.; Hogsett, W. E. (1987) Selection of the best exposure-response model using various
 9             7-hour ozone exposure statistics. Research Triangle Park, NC: U.S. Environmental Protection Agency,
10             Office of Air Quality Planning and Standards.
11
12     Lee, E. H.; Tingey, D. T.; Hogsett, W. E. (1988) Evaluation of ozone exposure indices in exposure-response
13             modeling. Environ. Pollut. 53: 43-62.
14
15     Lee, E. H.; Tingey, D. T.; Hogsett, W. E. (1989) Interrelation of experimental exposure and ambient air quality
16             data for comparison of ozone exposure indices and estimating agricultural losses. Corvallis, OR: U.S.
17             Environmental Protection Agency, Environmental Research Laboratory; EPA report no.
18             EPA-600/3-89-047. Available from: NTIS, Springfield, VA; PB89-195036.
19
20     Lee, W. S.; Chevone, B. I.; Seiler, J. R. (1990a) Growth and gas exchange of loblolly pine seedlings as
21             influenced by drought and air pollutants. Water Air Soil Pollut. 51: 105-116.
22
23     Lee, W. S.; Chevone, B. I.; Seiler, J. R. (1990b) Growth response and drought susceptibility of red spruce
24             seedlings exposed to simulated acidic rain and ozone. For.  Sci. 36: 265-275.
25
26     Lee, E. H.; Hogsett, W. E.; Tingey, D. T. (1991) Efficacy of ozone exposure indices in the standard setting
27             process.  In: Berglund, R. L.; Lawson, D. R.; McKee, D.  J., eds. Tropospheric ozone and the
28             environment: papers from an international conference; March 1990; Los Angeles, CA. Pittsburgh, PA:
29             Air & Waste Management Association; pp. 255-271. (A&WMA transaction series no. TR-19).
30
31     Lee, E. H.; Kramer, G. F.; Rowland, R. A.; Agrawal, M. (1992) Antioxidantsand growth regulators counter
32             the effects of O3 and SO2 in crop plants. Agric. Ecosyst. Environ. 38: 99-106.
33
34     Lee, E. H.; Hogsett, W. E.; Tingey, D. T. (1993a) Alternative attainment criteria for a secondary federal
35             standard for ozone. In: Nriagu, J. O., ed. Oxidants in the environment. New York, NY: John Wiley and
36             Sons: in press. (Advances in environmental sciences and technology series).
37
38     Lee, E. H.; Hogsett, E. H.; Tingey, D. T. (1993b)  Attainment and effects issues regarding the secondary ozone
39             air quality standard. In preparation.
40
41     Lefohn, A. S. (1984) A comparison of ambient ozone exposures for selected nonurban sites. Presented at: 77th
42             annual meeting of the Air Pollution Control  Association; June; San Francisco, CA. Pittsburgh, PA: Air
43             Pollution Control Association; paper no. 84-104.1.
44
45      Lefohn, A. S. (1988) Author's reply [a response to comments by Parry and Day, 1988]. Atmos. Environ.
46             22: 2058-2060.
47
48      Lefohn, A. S. (1992) Ozone standards and their relevance for protecting vegetation. In: Lefohn, A. S.,
49            ed. Surface level ozone exposures and their  effects on vegetation. Chelsea, MI: Lewis Publishers, Inc.;
50            pp. 325-359.
51
52     Lefohn, A. S.; Benedict, H. M. (1982) Development of a mathematical index that describes ozone concentration,
53            frequency and duration. Atmos. Environ.  16: 2529-2532.
54


         December 1993                               5-384       DRAFT-DO NOT QUOTE OR CITE

-------
 1     Lefohn, A. S.; Benkovitz, C. M. (1990) Air quality measurements and characterizations for vegetation effects
 2             research. In: Proceedings of the 83rd annual meeting of the Air and Waste Management Association;
 3             June; Pittsburgh, PA. Pittsburgh, PA:  Air and Waste Management Association; 90-98.1.
 4
 5     Lefohn, A. S.; Foley, J.  K. (1992) NCLAN results and their application to the standard-setting process:
 6             protecting vegetation from surface ozone exposures. J. Air Waste Manage. Assoc. 42: 1046-1052.
 7
 8     Lefohn, A. S.; Foley, J.  K. (1993) Establishing relevant ozone standards to protect vegetation and human health:
 9             exposure/dose-response considerations. J. Air Waste Manage. Assoc.  43:  106-112.
10
11     Lefohn, A. S.; Irving, P. M. (1988) Characterizing ambient ozone exposure regimes in agricultural areas.
12             In: Proceedings of the 81st annual meeting of the Air Pollution Control Association; June; Dallas, TX.
13             Pittsburgh, PA: Air Pollution Control  Association; 88-69.1.
14
15     Lefohn, A. S.; Jones, C. K.  (1986) The characterization of ozone and sulfur dioxide air quality data for assessing
16             possible vegetation effects.  J. Air Pollut. Control Assoc. 36: 1123-1129.
17
18     Lefohn, A. S.; Mohnen,  V. A. (1986) The characterization of ozone, sulfur dioxide, and nitrogen dioxide for
19             selected monitoring sites in the Federal Republic of Germany. J. Air Pollut. Control Assoc.
20             36: 1329-1337.
21
22     Lefohn, A. S.; Ormrod, D. P. (1984) A review and assessment of the effects of pollutant mixtures on
23             vegetation—research recommendations. Presented at: Vegetation effects workshop; April, 1983; Raleigh,
24             NC. Corvallis, OR: U.S. Environmental Protection Agency, Corvallis Environmental Research
25             Laboratory; EPA report no. EPA-600/3-84-037. Available from: NTIS, Springfield, VA;
26             PB84-177732/HSU.
27
28     Lefohn, A. S; Pinkerton, J. E. (1988) High resolution characterization of ozone data for sites located in forested
29             areas of the United States. JAPCA 38: 1504-1511.
30
31     Lefohn, A. S.; Runeckles, V. C. (1987) Establishing standards to protect vegetation—ozone exposure/dose
32             considerations. Atmos. Environ. 21: 561-568.
33
34     Lefohn, A. S.; Tingey, D. T. (1984) The co-occurrence of potentially phytotoxic concentrations of various
35             gaseous air pollutants. Atmos. Environ. 18: 2521-2526.
36
37     Lefohn, A. S.; Tingey, D. T. (1985) Comments on "Injury response of Phaseolus vulgaris to ozone flux
38             density." Atmos. Environ.  19: 206-207.
39
40     Lefohn, A. S.; Knudsen, H. P.; Logan,  J.  A.; Simpson, J.; Bhumralkar, C. (1987a) An evaluation of the kriging
41             method to predict 7-h seasonal mean ozone concentrations for estimating  crop losses. JAPCA
42             37: 595-602.
43
44     Lefohn, A. S.; Davis, C. E.; Jones, C. K.; Tingey, D. T.; Hogsett, W.  E. (1987b) Co-occurrence patterns of
45             gaseous air pollutant pairs at different  minimum concentrations in the  United States.  Atmos. Environ.
46             21: 2435-2444.
47
48     Lefohn, A. S.; Laurence, J.  A.; Kohut, R. J.  (1988a)  A comparison of indices that describe the relationship
49             between exposure to ozone and reduction in the yield of agricultural crops. Atmos. Environ.
50             22: 1229-1240.
51
52     Lefohn, A. S.; Laurence, J.  A.; Kohut, R. J.  (1988b) A comparison of indices that describe the relationship
53             between exposure to ozone and reduction in the yield of agricultural crops [response to comments by
54             V. C.  Runeckles]. Atmos. Environ. 22: 1242-1243.


         December  1993                               5-385       DRAFT-DO NOT QUOTE OR CITE

-------
 1     Lefohn, A. S.; Runeckles, V. C.; Krupa, S. V.; Shadwick, D. S. (1989) Important consideratins for establishing
 2            a secondary ozone standard to protect vegetation. JAPCA 39:  1039-1045.
 3
 4     Lefohn, A. S.; Krupa, S. V.; Winstanley, D. (1990) Surface ozone exposures measured at clean locations around
 5            the world.  Environ. Pollut. 63: 189-224.
 6
 7     Lefohn, A. S.; Shadwick,  D. S.; Foley, J.  K. (1991a) The quantification of surface-level ozone exposures across
 8            the United States. In: Berglund, R.  L.; Lawson, D. R.; McKee, D. J., eds. Tropospheric ozone and the
 9            environment: papers from an international conference; March  1990; Los Angeles, CA. Pittsburgh, PA:
10            Air & Waste Management Association; pp. 197-224. (A&WMA transaction series no. TR-19).
11
12     Lefohn, A. S.; Benkovitz, C. M.; Tanner,  R. L.; Smith, L. A.; Shadwick, D. S.  (1991b) Air quality
13            measurements and characterizations for terrestrial effects research. In: Irving, P. M., ed. Acidic
14            deposition: state of science and technology, volume I, emissions, atmospheric processes, and deposition.
15            Washington, DC: The U.S. National Acid Precipitation Assessment Program. (State of science and
16            technology report no. 7).
17
18     Lefohn, A. S.; Shadwick,  D. S.; Somerville, M. C.; Chappelka,  A. H.; Lockaby, B. G.; Meldahl, R. S.
19            (1992a) The characterization and comparision of ozone exposure indices used in assessing the response of
20            loblolly pine to ozone. Atmos. Environ. Part A 26: 287-298.
21
22     Lefohn, A. S.; Foley, J. K.; Spence, J.; Shadwick,  D. S. (1992b) Linking surface-level ozone exposures in the
23            United States with potential vegetation effects. In: Berglund, R. L., ed. Transactions of the tropospheric
24            ozone and the environment specialty conference II. Pittsburgh, PA: Air and Waste Management
25            Association; pp. 473-488.
26
27     Lefohn, A. S.; McEvoy, L. R.; Tingey, D. T.; Sebaugh, J. L.; Hogsett, W. E. (1993) Potential bias from
28            non-continuous monitoring of ambient ozone concentrations for characterizing hourly and daily 7- and
29             12-hour average concentrations. Atmos  Environ. Part A 27: 145-152.
30
31     Legge, A. H.; Savage, D. J.; Walker, R. B. (1978) Special techniques: B. a portable gas-exchange leaf chamber.
32            In: Heck, W. W.; Krupa, S. V.; Linzon, S. N., eds.  Methodology for the assessment of air pollution
33             effects on  vegetation: a handbook from a specialty conference; April; Minneapolis, MN. Pittsburgh, PA:
34             Air Pollution Control Association;  pp. 16-12—16-24.
35
36     Lenschow, D. H.; Pearson, R., Jr.; Stankov, B. B.  (1982) Measurement of ozone vertical flux to ocean and
37             forest. J.  Geophys. Res.  87: 8833-8837.
38
39     Leonardi, S.; Langebartels, C. (1990) Fall exposure of beech saplings (Fagus sylvatica L.)  to ozone and
40             simulated acid mist: effects on gas exchange and leachability. Water Air Soil Pollut. 54: 143-153.
41
42     Leone, I. A.; Brennan, E.  (1970) Ozone toxicity in tomato as modified by phosphorus nutrition. Phytopathology
43             60:  1521-1524.
44
45      Leone, I. A.; Brennan, E.; Daines, R. H.  (1966) Effect of nitrogen nutrition on the response of tobacco to ozone
46            in the atmosphere. J. Air Pollut. Control Assoc. 16: 191-196.
47
48     Lesser, V. M.; Rawlings, J. O.; Spruill, S. E.; Somerville,  M. C. (1990) Ozone effects on agricultural crops:
49            statistical methodologies and estimated dose-response relationships. Crop Sci. 30: 148-155.
50
51     Letham, D.  S.; Palni, L.  M. (1983) The biosynthesis and metabolism of cytokinins. Annu.  Rev. Plant Physiol.
52            34:  163-197.
53
          December  1993                               5-386       DRAFT-DO NOT QUOTE OR CITE

-------
  1      Leuning, R.; Neumann, H. H.; Thurtell, G. W. (1979a) Ozone uptake by corn (Lea mays L.): a general
  2             approach. Agric. Meteorol. 20:  115-135.
  3
  4      Leuning, R.; Unsworth, M. H.; Neumann, H. N.; King, K. M. (1979b) Ozone fluxes to tobacco and soil under
  5             field conditions. Atmos. Environ.  13: 1155-1163.
  6
  7      Levitt, J. (1972) Responses of plants to  environmental stresses. New York, NY: Academic Press. (Kozlowski,
  8             T. T., ed. Physiological ecology: a series of monographs, texts, and treatises).
  9
10      Lewis, E.; Brennan, E. (1977) A disparity in the ozone response of bean plants grown in a greenhouse, growth
11             chamber or open-top chamber. J. Air Pollut. Control Assoc. 27: 889-891.
12
13      Logan, J. A. (1989) Ozone in rural areas of the United  States. J. Geophys. Res. 94: 8511-8532.
14
15      Long, R. P.; Davis, D. D.  (1991) Black cherry growth  response to ambient ozone and EDU. Environ. Pollut.
16             70: 241-254.
17
18      Loomis, J.;  Lockwood, M.; DeLacy,  T. (1993) Some empirical evidence on embedding  effects in contingent
19             valuation. J. Environ. Econ. Manage. 24: 45-55.
20
21      Losch, R.; Tenhunen, J. D. (1981) Stomatal responses to humidity—phenomenon and mechanism. In: Jarvis,
22             P. G.; Mansfield, T. A., eds. Stomatal physiology; pp. 137-161. (Society for Experimental Biology
23             seminar series no. 8).
24
25      Lucas, P. W.; Cottam, D. A.; Sheppard, L. J.; Francis, B. J. (1988) Growth responses  and delayed winter
26             hardening in Sitka spruce following summer exposure to ozone. New Phytol.  108: 495-504.
27
28      Ludwig, F.  L.; Shelar, E.,  Jr. (1980) Empirical relationships between observed ozone concentrations and
29             geographical areas with concentrations likely to  be above 120 ppb. J. Air Pollut. Control Assoc.
30             30: 894-897.
31
32      Luethy-Krause, B.; Landolt, W. (1990)  Effects of ozone on starch accumulation in Norway spruce (Picea abies).
33             Trees 4: 107-110.
34
35      Lutz, C.; Heinzmann, U.; Gulz, P. G. (1990) Surface structures and epicuticular wax composition of spruce
36             needles after long-term treatment with ozone and acid mist. Environ.  Pollut. 64:  313-322.
37
38      Luxmoore, R. J. (1988) Assessing the mechanisms of crop loss from air pollutants with process models.
39            In: Heck, W. W.; Taylor, O.  C.; Tingey, D. T., eds.  Assessment of crop loss from air pollutants.
40            New York, NY: Elsevier Applied  Science; pp. 417-444.
41
42      MacDowall, F. D. H. (1965) Predisposition of tobacco to ozone damage. Can. J. Plant Sci. 45: 1-12.
43
44      Macdowall,  F. D. H.; Cole, A. F. W. (1971) Threshold and synergistic damage to tobacco by ozone and sulfur
45            dioxide. Atmos. Environ. 5: 553-559.
46
47      MacDowall, F. D. H.; Mukammal, E. I.;  Cole, A.  F. W. (1964) Direct correlation of air polluting ozone and
48            tobacco weather fleck. Can. J. Plant Sci. 44: 410-417.
49
50      Mackay, C.  E.; Senaratna, T.; McKersie,  B.  D.; Fletcher, R. A. (1987) Ozone induced injury to cellular
51            membranes in Triticum aestivum L. and protection by the triazole S-3307. Plant Cell Physiol.
52            28: 1271-1278.
53
        December 1993                               5.387       DRAFT-DO NOT QUOTE OR CITE

-------
  1     MacLean, D.  C. (1990) Joint action of ozone and hydrogen fluoride on foliar senescence in maize. Environ.
  2            Pollut. 63: 283-292.
  3
  4     Madamanchi,  N. R.; Hausladen, A.; Alscher, R. G.; Amundson, R. G.;  Fellows, S. (1991) Seasonal changes in
  5            antioxidants in red spruce (Picea ruhens Sarg.) from three field sites in the northeastern United States.
  6            New Phytol. 118:331 -338.
  7
  8     Madamanchi,  N. R.; Anderson, J. V.; Alscher, R. G.; Cramer, C. L.; Hess, J. L. (1992) Purification of
  9            multiple forms of glutathione reductase  from pea (Pisum sativum L.) seedlings and enzyme levels in
10            ozone-fumigated pea leaves.  Plant Physiol. 100: 138-145.
11
12     Magel, E.; H611, W.; Ziegler, H. (1990) Alteration of physiological parameters in needles of cloned spruce trees
13            (Picea abies (L.) Karst.) by  ozone and acid mist.  Environ. Pollut. 64: 337-345.
14
15     Mahoney, M.  J.; Chevone, B. I.; Skelly, J.  M.; Moore, L. D. (1985) Influence of mycorrhizae on the growth of
16            loblolly pine seedlings exposed to ozone and sulfur dioxide. Phytopathology 75: 679-682.
17
18     Makansi, M. (1986)  Effect of ageing on dyeability of nylon yarns. Text. Chem. Color. 18(1): 27-35.
19
20     Mandl, R. H.; Weinstein,  L. H.; McCune, D. C.; Keveny, M. (1973) A cylindrical, open-top chamber for the
21            exposure of plants to air pollutants in the field.  J. Environ. Qual. 2: 371-376.
22
23     Mandl, R. H.; Laurence, J. A.; Kohut, R. J. (1989) Development and testing of open-top chambers for exposing
24            large,  perennial plants to air pollutants.  J.  Environ. Qual. 18: 534-540.
25
26     Mann, L. K.;  McLaughlin, S. B.; Shriner, D. S. (1980) Seasonal physiological responses of white pine under
27            chronic air pollution stress. Environ. Exp. Bot. 20: 99-105.
28
29     Manning, W.  J.; Keane, K. D.  (1988) Effects of air pollutants on interactions between plants, insects, and
30            pathogens. In: Heck, W. W.; Taylor, O. C.; Tingey, D. T., eds. Assessment of crop  loss from air
31            pollutants.  London, United Kingdom: Elsevier Applied Science; pp. 365-386.
32
33     Manning, W.  J.; Feder, W. A.; Perkins, I.; Glickman, M. (1969) Ozone injury and infection  of potato leaves by
34            Botrytis cinerea. Plant Dis. Rep.  53: 691-693.
35
36     Manning, W.  J.; Feder, W. A.; Papia, P. M.; Perkins, I. (1971a) Effect of low levels of ozone on growth and
37            susceptibility of cabbage plants to Fusarium oxysporum F.  sp. conglutinans. Plant Dis. Rep. 55: 47-49.
38
39     Manning, W.  J.; Feder, W. A.; Papia, P. M.; Perkins, I. (197Ib) Influence of foliar ozone injury on root
40            development and root surface fungi of pinto bean  plants. Environ. Pollut. 1: 305-312.
41
42     Mansfeld, F. (1980)  Regional air pollution study:  effects of airborne sulfur pollutants on materials. Research
43            Triangle Park,  NC: U.S. Environmental Protection Agency, Environmental Sciences Research
44            Laboratory; EPA report no.  EPA-600/4-80-007. Available from: NTIS, Springfield, VA;  PB81-126351.
45
46     Mansfield, T.  A.; McCune, D.  C. (1988) Problems of crop loss assessment when there is exposure to two or
47            more gaseous pollutants. In:  Heck, W. W.; Taylor, O. C.; Tingey, D. T.,  eds. Assessment of crop loss
48            from air pollutants. London, United Kingdom: Elsevier Applied Science; pp. 317-344.
49
50     Martin, B.; Bytnerowicz, A.; Thorstenson, Y. R.  (1988)  Effects of air pollutants on the composition of stable
51            carbon isotopes, 5  C, of leaves and wood, and on leaf injury. Plant Physiol. 88:  218-223.
52
53     Matsui, M.; Koike, T.; Shibata, K.  (1988) Ozone fading of phenolphthalein and aurin. J.  Soc. Dyers Colour
54            104: 482-486.


         December 1993                              5-388      DRAFT-DO NOT QUOTE OR CITE

-------
  1      Matsushima, J.; Yonemori, K.; Iwao, K. (1985) Sensitivity of satsuma mandarin to ozone as related to stomatal
  2             function indicated by transpiration rate, change of stem diameter, and leaf temperature. J. Am. Soc.
  3             Hortic. Sci. 110: 106-108.
  4
  5      Matyssek, R.; Gunthardt-Goerg, M. S.; Saurer, M.; Keller, T. (1992) Seasonal growth, 613C in leaves and stem,
  6             and phloem structure of birch (Betula pendula) under low ozone concentrations. Trees 6: 69-76.
  7
  8      Matyssek, R.; Keller, T.; Koike, T. (1993) Branch growth and leaf gas exchange of Populus tremuloides exposed
  9             to low ozone concentrations throughout two growing seasons. Environ. Pollut. 79: 1-7.
 10
 11      McCool, P. M. (1988) Effect of air pollutants on mycorrhizae. In:  Schulte-Hostede, S; Darrall, N. M.; Blank,
 12             L.  W.; Wellburn, A. R., eds. Air pollution and plant metabolism. London, United Kingdom:  Elsevier
 13             Applied Science; pp. 356-365.
 14
 15      McCool, P. M.; Menge, J.  A. (1984) Interaction of ozone and mycorrhizal fungi on tomato as influenced by
 16             fungal species and host variety. Soil Biol. Biochem. 16: 425-427.
 17
 18      McCool, P. M.; Musselman, R. C. (1990) Impact of ozone on growth of peach, apricot,  and almond.
 19             Hortscience 25: 1384-1385.
 20
 21      McCool, P. M.; Menge, J.  A.; Taylor, O. C. (1982) Effect of ozone injury and light stress on response of
 22             tomato to infection by the vesicular-arbuscular mycorrhizal  fungus, Glomus fasciculatus. J. Am. Soc.
 23             Hortic. Sci. 107: 839-842.
 24
 25      McCool, P. M.; Musselman, R. C.; Teso, R. R. (1987) Air pollutant yield-loss assessment for four vegetable
 26             crops. Agric. Ecosyst. Environ. 20: 11-21.
 27
 28      McCool, P. M.; Musselman, R. C.; Younglove, T.; Teso, R. R. (1988) Response of kidney bean to sequential
 29             ozone exposures. Environ. Exp. Bot. 28: 307-313.
 30
 31      McGartland, A. M. (1987) The implications of ambient ozone standards for U.S. agriculture: a comment and
 32             some further evidence. J. Environ. Manage. 24: 139-146.
 33
 34      Mcllveen, W.  D.; Spotts, R. A.; Davis, D. D. (1975) The influence of soil zinc on nodulation, mycorrhizae,  and
 35             ozone-sensitivity of Pinto bean. Phytopathology 65: 645-647.
 36
 37      McLaughlin, S. B.; Taylor, G. E. (1981) Relative humidity: important modifier of pollutant uptake by plants.
 38             Science (Washington,  DC) 211:  167-169.
 39
 40      McLaughlin, S. B.; McConathy, R. K.; Duvick, D.; Mann, L. K.  (1982) Effects of chronic air pollution stress
 41             on  photosynthesis, carbon allocation, and growth of white pine trees. For. Sci. 28: 60-70.
 42
 43      McLeod, A. R.; Fackrell, J. E.; Alexander, K. (1985) Open-air fumigation of field crops: criteria and design  for
 44             a new  experimental  system. Atmos. Environ. 19: 1639-1649.
 45
 46      McLeod, A. R.; Shaw, P. J. A.;  Holland, M. R. (1992) The  Liphook Forest Fumigation Project: studies of
 47             sulphur dioxide and ozone effects on coniferous trees. For.  Ecol. Manage. 51: 121-127.
48
49      McQuattie, C. J.;  Schier, G. A. (1992) Effect of ozone and aluminum on pitch pine (Pinus rigida) seedlings:
50             anatomy of mycorrhizae.  Can. J. For. Res. 22: 1901-1916.
51
52      Mebrahtu, T.;  Rangappa, M.; Benepal, P. S. (1988) Inheritance study of common bean (Phaseolus vulgaris L.)
53             to ambient O3 injury. Annual report of the Bean Improvement Cooperative: v.  31; pp. 108-109.
54


         December 1993                               5.339        DRAFT-DO NOT QUOTE  OR CITE

-------
  1      Mebrahtu, T.; Mersie, W.; Rangappa, M. (1990a) Generation mean analysis of inheritance of insensitivity to
  2             ozone injury in two crosses of beans (Phaseolus vulgaris L.). J- Hort. Sci. 65: 19-24.
  3
  4      Mebrahtu, T.; Mersie, W.; Rangappa, M. (1990b) Inheritance of ambient ozone insensitivity in common bean
  5             (Phaseolus vulgaris L.). Environ. Pollut. 67: 79-89.
  6
  7      Mebrahtu, T.; Mersie, W.; Rangappa, M. (1990c) A seven-parental diallel analysis of ozone insensitivity in
  8             common beans. J.  Genet. Breed. 44: 69-74.
  9
10      Mehlhorn, H.; Wellburn, A. R. (1987) Stress ethylene formation determines plant sensitivity to ozone. Nature
11             (London) 327: 417-418.
12
13      Mehlhorn, H.; Seufert, G.; Schmidt, A.; Kunert, K. J. (1986) Effect of SO2 and O3 on production of
14             antioxidants in conifers. Plant Physiol. 82: 336-338.
15
16      Mehlhorn, H.; O'Shea, J.  M.;  Wellburn, A. R. (1991) Atmospheric ozone interacts with stress ethylene
17             formation by plants to cause visible plant injury. J. Exp. Hot. 42:  17-24.
18
19      Meier, S.; Grand, L. F.; Schoeneberger, M. M.; Reinert, R. A.; Bruck, R. I.  (1990) Growth, ectomycorrhizae
20             and nonstructural carbohydrates of loblolly pine seedlings exposed to ozone and soil water deficit.
21             Environ. Pollut. 64:  11-27.
22
23      Meiners, J. P.; Heggestad, H.  E. (1979) Evaluation of snap bean cultivars for resistance to ambient oxidants in
24             field plots and to ozone in chambers. Plant Dis. Rep. 63: 273-277.
25
26      Mendelsohn,  R.; Markstrom, D. (1988) The use of travel cost and hedonic methods in assessing environmental
27             benefits. In: Peterson, G. L.;  Driver, B. L.; Gregory, R., eds. Amenity resource valuation: integrating
28             economics with other disciplines. State College, PA: Venture Publishing, Inc.; pp. 160-166.
29
30      Menser, H. A.; Heggestad, H. E. (1966) Ozone and sulfur dioxide synergism:  injury  to tobacco plants. Science
31             (Washington, DC) 153: 424-425.
32
33      Menser, H. A.; Hodges, G.  H. (1967) Nitrogen nutrition and susceptibility of tobacco leaves to ozone. Tobacco
34             Sci. 11:  151-154.
35
36      Menser, H. A.; Hodges, G.  H. (1968) Varietal tolerance of tobacco to ozone dose rate. Agron. J. 60: 349-352.
37
38      Menser, H. A.; Street, O.  E. (1962) Effects of air pollution, nitrogen levels, supplemental irrigation, and plant
39             spacing on weather fleck and leaf losses of Maryland tobacco. Tobacco 155: 192-196.
40
41      Mersie, W.; Mebrahtu, T.; Rangappa, M. (1989) Ozone interactions on corn (Zea mays), bean (Phaseolus
42             vulgaris), and soybean (Glycine max).  Weed Tech. 3:  650-653.
43
44      Mersie, W.; Mebrahtu, T.; Rangappa, M. (1990a) Evaluation of bean introductions for ozone insensitivity.
45             HortScience 25: 1581-1582.
46
47      Mersie, W.; Mebrahtu, T.; Rangappa, M. (1990b) Response of corn to combinations  of atrazine, propyl gallate
48             and ozone. Environ. Exp. Bot. 30:  443-449.
49
50     Meyer, D. A.; Sommer, J. G.  (1957) The development of weather and aging resistant pneumatic tires and
51             mechanical rubber goods:  final technical report. Dayton, OH: The Dayton Rubber Company; contract
52             no. DA-20-089-ORD-36756. Available from: NTIS, Springfield, VA; AD-142212.
53
         December 1993                              5-390       DRAFT-DO NOT QUOTE OR CITE

-------
 1     Middleton, J. T.; Kendrick, J. B., Jr.; Schwalm, H. W. (1950) Injury to herbaceous plants by smog or air
 2            pollution. Plant Dis. Rep. 34: 245-252.
 3
 4     Millan, M. M.; Artinano, B. (1992) Mesometeorological cycles of air pollution in the Iberian peninsula.
 5            Brussels,  Belgium: Commission of European Communities, Environmental Research Programme; report
 6            no. 44.
 7
 8     Miller, P. R.; Grulke, N. E. (1993) Effects of air pollution on giant sequoia ecosystems Washinton, DC: USDA
 9            Forest Service; general technical report.
10
11     Miller, P. R.; McBride, J. R. (1989) Trends of ozone damage to conifer forests in the western U.S.A.,
12            particularly southern California. In: Bucher, J. B.; Bucher-Wallin, I., eds. Air pollution and forest
13            decline: vols. I and II; 14th international meeting for specialists in air pollution effects on forest
14            ecosystems; October,  1988; Interlaken, Switzerland. Birmensdorf, Switzerland:  Eidgenoessische Anstalt
15            Fuer das Forstliche Versuchswesen (EAFV); pp. 61-68.
16
17     Miller, J. E.; Pursley, W. A.  (1990) Effects of ozone and UV-B radiation on growth, UV-B absorbing pigments,
18            and antioxidants in soybean. Plant Physiol. 93(suppl. 1):  101.
19
20     Miller, P. R.; Parmeter, J. R., Jr.; Flick, B. H.; Martinez, C. W. (1969) Ozone dosage response of ponderosa
21            pine seedlings. J. Air  Pollut. Control Assoc. 19: 435-438.
22
23     Miller, P. R.; McCutchan, M. H.;  Ryan, B. C. (1972) Influence of climate and topography on oxidant air
24            pollution concentrations that damage conifer forests in southern California. Mitt. Forst.
25            Bundesversuchsanst. Wien 97: 585-607.
26
27     Miller, V. L.; Howell, R. K.; Caldwell, B. E. (1974) Relative sensitivity of soybean genotypes to ozone and
28            sulfur dioxide. J. Environ.  Qual. 3: 35-37.
29
30     Miller, P. M.; Tomlinson, H.; Taylor, G.  S. (1976) Reducing severity of ozone damage to tobacco and beans by
31            combining benomyl or carboxin with contact nematicides. Plant Dis. Rep. 60: 433-436.
32
33     Miller, P. R.; Taylor, O. C.; Wilhour, R. G.  (1982) Oxidant air pollution  effects on a  western coniferous forest
34            ecosystem. Corvallis,  OR:  U.S. Environmental Protection Agency,  Environmental Research Laboratory;
35            EPA report no. EPA-600/D-82-276. Available from: NTIS, Springfield, VA; PB83-189308.
36
37     Miller, P. R.; Longbotham, G. J.;  Longbotham, C. R. (1983) Sensitivity of selected western conifers to ozone.
38            Plant Dis. 67: 1113-1115.
39
40     Miller, P. R.; Taylor, O. C.; Poe,  M. P. (1986) Spatial variation of summer ozone concentrations in the
41            San Bernardino mountains.  Presented at: 79th annual meeting of the Air Pollution Control Association;
42            June; Minneapolis, MN. Pittsburgh, PA: Air Pollution Control Association; paper no. 86-39.2.
43
44     Miller, J. E.; Patterson, R. P.;  Heagle, A. S.; Pursley, W. A.; Heck, W. W. (1988) Growth of cotton under
45            chronic ozone stress at two levels of soil moisture. J. Environ. Qual.  17: 635-643.
46
47     Miller, P. R.; McBride, J. R.; Schilling, S. L.; Gomez, A. P. (1989a) Trend of ozone  damage to conifer forests
48            between 1974 and 1988 in the San Bernardino mountains in southern California. In: Olson,  R. K.;
49            Lefohn, A. S., eds. Effects of air pollution on western forests. Pittsburgh, PA:  Air and Waste
50            Management Association; pp. 309-324 (Transactions series no. 16).
51
52     Miller, J. E.; Heagle, A. S.; Vozzo, S. F.; Philbeck, R. B.; Heck, W. W. (1989b) Effects of ozone and water
53            stress, separately and  in combination, on soybean yield. J. Environ. Qual. 18: 330-336.
54


         December 1993                               5-391       DRAFT-DO NOT QUOTE OR CITE

-------
 1     Miller, J. E.; Patterson, R. P.; Pursley, W. A.; Heagle, A. S.; Heck, W. W. (1989c) Response of soluble
 2            sugars and starch in field-grown cotton to ozone, water stress, and their combination. Environ. Exp. Bot.
 3            29: 477-486.
 4
 5     Miller, J. E.; Pursley, W. A.; Vozzo, S. F.; Heagle, A. S. (1991a) Response of net carbon exchange rate of
 6            soybean to ozone at different stages of growth and its relation to yield. J. Environ. Qual. 20: 571-575.
 7
 8     Miller, P. R.; McBride, J. R.; Schilling, S. L. (1991b) Chronic ozone injury and associated stresses affect
 9            relative competitive capacity of species comprising the California mixed conifer forest type. In: Memorias
10            del primer simposial nacional; Agriculture sostenible: Una opcion para desarollo sin deterioro ambiental.
11            Montecillo, Edo. Mexico, Mexico: Comision de Estudios Ambientales, Colegio de Postgraduados;
12            pp. 161-172.
13
14     Miller, P. R.; de  Bauer, M.;  Nolasco Quevada, A.; Hernandez-Tejeda, T. (1993) Ozone exposure characteristics
15            of forests near Mexico City and Los Angeles.  Atmos. Environ.: submitted.
16
17     Mitchell, R. C.; Carson, R. T. (1989) Using surveys to value public goods: the contingent valuation method.
18            Washington, DC: Resources for the Future.
19
20     Moldau,  H.;  Sober, J.; Sober, A. (1990) Differential sensitivity of stomata and mesophyll to sudden exposure of
21            bean  shoots to ozone. Photosynthetica 24: 446-458.
22
23     Moldau,  H.;  Kull, O.; Sober, J.; Norby, R. J. (1991a) Differential response of carbon dioxide uptake parameters
24            of soil- and sand-grown Phaseolus vulgaris (L.) plants to absorbed ozone flux. Environ. Pollut.
25            74: 251-262.
26
27     Moldau, H.;  Sober, J.; Karolin, A.; Kail is, A. (1991b) CO2 uptake and respiration losses in vegetative bean
28            plants due to ozone absorption. Photosynthetica 25: 341-349.
29
30     Monteith, J. L.; Unsworth, M. H. (1990) Principles of environmental physics. 2nd ed. London, United
31            Kingdom: Edward Arnold; pp. 250-254.
32
33     Monies,  R. A.; Blum, U.; Heagle, A. S.  (1982) The effects of ozone and nitrogen fertilizer on tall fescue, ladino
34            clover, and a fescue-clover mixture. I. Growth, regrowth, and forage production. Can. J. Bot.
35            60: 2745-2752.
36
37     Moore, R. A. F.; Ruetsch, S. B.; Weigmann, H.-D. (1984) The role of dye diffusion in the ozone fading of acid
38            and disperse dyes in polyamides. Text. Chem. Color. 16(12): 23-29.
39
40     Morey, E.; Shaw, W. D.; Rowe, R. D. (1991) A discrete-choice model of recreational participation, site choice,
41             and activity valuation when complete trip data are not available. J. Environ. Econ. Manage. 20: 181-201.
42
43     Morris,  M. A. (1966) Effect  of weathering on cotton fabrics. Davis, CA: Western Regional Research
44             Cooperative Project;  California Agricultural Experiment Station bulletin no. 823.
45
46     Mortensen, L.  (1990a) Effects of ozone on growth and dry matter partitioning in different provenances of
47             Norway spruce  (Plcea ables L. Karst.). Norw. J.  Agric. Sci. 4: 37-342.
48
49      Mortensen, L.  M. (1990b) The effects of low O3 concentrations on growth of Triticum aestivum L. at different
50            light and air humidity levels. Norw. J. Agric. Sci. 4: 337-342.
51
52     Mortensen, L.  M. (1990c) Effects of ozone on growth of Triticum aestivum L. at different light, air humidity,
53            and CO2 levels. Norw. J. Agric.  Sci. 4: 343-348.
54


         December 1993                               5-392       DRAFT-DO NOT QUOTE OR CITE

-------
  1      Mortensen, L. M. (1992a) Effects of ozone on growth of seven grass and one clover species. Acta Agric. Scand.
  2             Sect. B Soil Plant Sci. 42: 235-239.
  3
  4      Mortensen, L. M. (1992b) Effects of ozone concentration on growth of tomato at various light, air humidity, and
  5             carbon dioxide levels. Sci. Hortic. (Amsterdam) 49: 17-24.
  6
  7      Mortensen, L. M.; Nilsen, J. (1992) Effects of ozone and temperature on growth of several wild plant species.
  8             Norw. J. Agric. Sci. 6:  195-204.
  9
10      Mortensen, L. M.; Skre, O.  (1990) Effects of low ozone concentrations on growth of Betula pubescens Ehrh.,
11             Betula verrucosa Ehrh, and Alnus incana  L. Moench.  New  Phytol. 115: 165-170.
12
13      Moser, T. J.; Tingey, D. T.; Rodecap, K. D.; Rossi, D. J.; Clark, C. S. (1988) Drought stress applied during
14             the reproductive phase reduced ozone-induced effects in bush bean. In: Heck, W. W.; Taylor, O. C.;
15             Tingey, D. T., eds. Assessment of crop loss from air pollutants. London, United Kingdom:  Elsevier
16             Applied Science; pp. 345-364.
17
18      Mudano, J. E.; Allen, H. L.; Kress, L. W. (1992) Stem and foliage elongation of young loblolly pine as affected
19             by ozone. For. Sci. 38:  324-335.
20
21      Mueller, W.  J.; Stickney, P. B. (1970) A survey and economic assessment of the effects of air pollution on
22             elastomers: final report. Columbus, OH: Battelle Memorial Institute, Columbus Laboratories; National
23             Air Pollution Control Administration contract no. CPA-22-69-146.
24
25      Mulcahy, D. L. (1979) The rise of the angiosperms: a genecological factor. Science (Washington, DC)
26             206:  20-23.
27
28      Mulcahy, D. L.; Mulcahy, G. B. (1983) Pollen selection: an overview. In: Mulcahey, D. L.; Ottaviano, E.,
29             eds. Pollen: biology and implications for plant breeding. New York,  NY: Elsevier Science Publishers;
30             pp. xv-xvii.
31
32      Mulchi, C. L.;  Sammons, D. J.; Baenziger, P. S. (1986) Yield and grain quality responses of soft red winter
33             wheat exposed to ozone during anthesis. Agron. J.  78: 593-600.
34
35      Mulchi, C. L.;  Lee, E.; Tuthill, K.; Olinick, E. V. (1988) Influence of ozone stress on growth processes yields
36             and grain quality characteristics among soybean cultivars. Environ. Pollut. 53: 151-170.
37
38      Mulchi, C. L.;  Slaughter, L.; Saleem, M.; Lee, E. H.; Pausch, R.; Rowland, R. (1992) Growth and
39             physiological characteristics of soybean in open-top chambers in response to ozone and increased
40             atmospheric CC^. Agric. Ecosyst. Environ. 38: 107-118.
41
42      Mumford, R. A.; Lipke, H.; Laufer, D.  A.; Feder, W. A. (1972) Ozone-induced changes in corn pollen.
43             Environ. Sci. Technol. 6: 427-430.
44
45      Munasinghe, M. (1992) Water supply and environmental management: developing world applications.
46             San Francisco, CA: Westview Press.
47
48      Munn, R. E. (1970) Biometeorological methods. New York, NY: Academic  Press.
49
50      Murray, J. J.; Howell, R. K.; Wilton, A. C. (1975) Differential response of seventeen Poa pratensis cultivars to
51             ozone and sulfur dioxide. Plant Dis. Rep.  59: 852-854.
52
         December 1993                               5.393       DRAFT-DO NOT QUOTE OR CITE

-------
 1     Murray, D. R.; Atwater,  M. A.; Yocom, J. E. (1985) Assessment of material damage and soiling from air
 2            pollution in the South Coast Air Basin. Sacramento, CA: California State Air Resources Board; report
 3            no. ARB-R-86/282. Available from: NTIS, Springfield, VA; PB86-232840/XAB.
 4
 5     Musselman, R. C.; Melious, R. E. (1984) Sensitivity of grape cultivars to ambient ozone. HortScience
 6            19: 657-659.
 7
 8     Musselman, R. C.; Taschenberg, E.  F. (1985) Usefulness of vineyard fungicides as antioxidants for grapevines.
 9            Plant Dis. 69: 406-408.
10
11     Musselman, R. C.; Oshima, R. J.; Gallavan, R. E. (1983) Significance of pollutant concentration distribution in
12            the response of 'red kidney' beans to ozone. J. Am. Soc. Hortic. Sci.  108: 347-351.
13
14     Musselman, R. C.; Forsline, P. L.; Render, W. J. (1985) Effects of sulfur dioxide and ambient ozone on
15            concord grapevine growth and productivity. J. Am. Soc. Hortic. Sci.  110: 882-888.
16
17     Musselman, R. C.; McCool, P. M.;  Oshima,  R. J.; Teso, R. R. (1986a) Field chambers for assessing crop loss
18            from  air pollutants. J. Environ. Qual.  15:  152-157.
19
20     Musselman, R. C.; Huerta,  A.  J.; McCool, P. M.; Oshima, R. J. (1986b) Response of beans to simulated
21            ambient and uniform ozone distributions with equal peak concentration. J. Am. Soc. Hortic. Sci.
22            111:470-473.
23
24     Musselman, R. C.; McCool, P. M.;  Younglove, T. (1988) Selecting ozone exposure statistics for determining
25            crop yield loss from air pollutants. Environ. Pollut. 53: 63-78.
26
27     Nast, W.; Mortensen, L.; Fischer, K.; Fitting, I.  (1993) Effects of air pollutants on the growth and antioxidative
28            system of Norway spruce exposed in open-top chambers. Environ. Pollut. 80: 85-90.
29
30     Neighbour, E. A.; Pearson, M.; Mehlhorn, H. (1990) Purafil-filtration prevents the development of
31            ozone-induced frost injury: a potential role for nitric oxide. Atmos. Environ. Part A 24: 711-715.
32
33     Niese, J. N.; Strong, T. F.  (1992) Economic  and  tree diversity trade-offs in managed northern hardwoods. Can.
34            J. For. Res. 22: 1807-1813.
35
36     Nipe, M. R.  (1981) Atmospheric contaminant fading. Text. Chem. Color.  13: 136-146.
37
38     Norby, R. J.; Richter, D. D.; Luxmoore, R.  J. (1985) Physiological processes in soybean inhibited by gaseous
39            pollutants but not by acid rain. New Phytol. 100: 79-85.
40
41     Norby, R. J.; Takemoto, B. K.; Johnston, J.  W.; Shriner, D. S. (1986) Acetylene reduction rate as a
42            physiological indicator  of the response of  field-grown soybeans to simulated acid rain and ambient
43            gaseous pollutants. Environ.  Exp. Bot. 26: 285-290.
44
45      Norton, B. G. (1987) Why preserve  natural variety? Princeton, NJ: Princeton University Press.
46
47      Nouchi, I.; Aoki, K.  (1979) Morning glory as a photochemical oxidant indicator. Environ.  Pollut. 18: 289-303.
48
49     Nouchi, I.; Mayumi,  H.; Yamazoe,  F. (1984) Foliar injury response of petunia and kidney bean to simultaneous
50            and alternate exposures to ozone and  PAN.  Atmos. Environ.  18: 453-460.
51
52     Nouchi, I.; Ito, O.; Harazono, Y.; Kobayashi, K. (1991) Effects of chronic ozone exposure on growth root
53            respiration and nutrient uptake of rice plants. Environ. Pollut. 74: 149-164.
54


         December 1993                               5-394       DRAFT-DO NOT QUOTE OR CITE

-------
 1     O'Gara, P. J. (1922) Sulfur dioxide and fume problems and their solution, (presented at the 14th semiannual
 2            meeting of the American Institute of Chemical Engineers, Niagara Falls, Canada, June 19-22, 1922).
 3            Presented at: 14th semiannual meeting of the American Institute of Chemical Engineers; June; Niagara
 4            Falls, Canada. Proceedings and papers of the meeting summarized in J. Ind. Eng. Chem.  14: 744-745 by
 5            J. C. Olsen.
 6
 7     Odum, E. P. (1963) Ecology. New York,  NY: Holt, Rinehart and Winston.
 8
 9     Okano, K.; Ito, O.; Takeba, G.; Shimizu, A.; Totsuka, T. (1985) Effects of ©3 and NO2 alone or in
10            combination on the distribution of l C-assimilate in kidney bean plants. Jpn. J. Crop Sci. 54: 152-159.
11
12     Oliver, C. D.; Larson,  B. C. (1991) Forest stand dynamics. New York, NY: McGraw-Hill.
13
14     Olsen, A. (1989) The economic value of hunting and fishing in Montana. Trans. North Am. Wildl. Nat. Resour.
15            Conf. 54: 239-246.
16
17     Olsen, D.; Richards, J.; Scott, R.  D. (1991) Existence and sport values for doubling the size of Columbia River
18            basin salmon and steelhead runs. Rivers 2:  44-56.
19
20     Olszyk, D. M.; Tibbitts, T. W. (1981) Stomatal  response and leaf injury of Pisum sativum L. with SO2 and
21            O3 exposures: I. influence of pollutant level and leaf maturity. Plant Physiol. 67: 539-544.
22
23     Olszyk, D. M.; Bytnerowicz, A.; Kats, G.; Dawson, P. J.; Wolf, J.; Thompson,  C. R. (1986a) Crop effects
24            from air pollutants in air exclusion systems vs. field chambers.  J. Environ. Qual.  15: 417-422.
25
26     Olszyk, D. M.; Bytnerowicz, A.; Kats, G.; Dawson, P. J.; Wolf, J.; Thompson,  C. R. (1986b) Effects of sulfur
27            dioxide and ambient ozone on winter wheat and lettuce. J. Environ. Qual. 15: 363-369.
28
29     Olszyk, D. M.; Maas, E. V.; Kats, G.; Francois, L. E. (1988) Soil salinity and ambient ozone: lack of stress
30            interaction for field-grown alfalfa. J. Environ. Qual.  17: 299-304.
31
32     Olszyk, D. M.; Dawson, P. J.; Morrison, C. L.; Takemoto, B. K. (1990a) Plant response to nonfiltered air vs.
33            added ozone generated from dry air or oxygen. J. Air Waste Manage. Assoc. 40: 77-81.
34
35     Olszyk, D. M.; Kats, G.; Morrison, C. L.; Dawson, P. J.; Gocka, I.;  Wolf, J.; Thompson, C. R. (1990b)
36             'Valencia' orange fruit yield with ambient oxidant or sulfur dioxide exposures. J. Am. Soc. Hortic.  Sci.
37             115: 878-883.
38
39     Olszyk, D.; Bytnerowicz, A.; Kats, G.; Reagan, C.; Hake, S.; Kerby, T.; Millhouse, D.; Roberts, B.;
40            Anderson, C.; Lee, E. H. (1993) Cotton yield losses and ambient ozone concentrations in California's
41            San Joaquin Valley. J.  Environ. Qual.: in press.
42
43     Ormrod, D. P.  (1976) Sensitivity of pea cultivars to ozone. Plant Dis. Rep. 60: 423-426.
44
45     Ormrod, D. P.; Kemp, W.  G.  (1979) Ozone response of tomato plants infected with cucumber mosaic virus
46            and/or tobacco mosaic  virus. Can. J. Plant Sci. 59:  1077-1083.
47
48     Ormrod, D. P.; Adedipe, N. O.; Hofstra, G. (1971) Responses of cucumber, onion and potato cultivars to
49            ozone. Can. J.  Plant Sci. 51: 283-288.
50
51     Ormrod, D. P.; Adedipe, N. O.; Hofstra, G. (1973) Ozone effects on growth of radish plants as influenced by
52            nitrogen and phosphoris nutrition and by temperature. Plant Soil 39: 437-439.
53
         December 1993                               5.395       DRAFT-DO NOT QUOTE OR CITE

-------
 1     Ormrod, D. P.; Marie, B. A.; Allen, O. B. (1988) Research approaches to pollutant crop loss functions.
 2             In: Heck, W. W.; Taylor, O. C.; Tingey, D. T.,  eds. Assessment of crop loss from air pollutants.
 3             New York, NY: Elsevier Applied Science; pp. 27-44.
 4
 5     Oshima, R. J. (1978) The impact of sulfur dioxide on vegetation: a sulfur dioxide-ozone response model: final
 6             report. Riverside, CA: University of California, Statewide Air Pollution Research Center; ARB
 7             agreement no. A6-162-30. Available from: NTIS, Springfield, VA; PB-283604.
 8
 9     Oshima, R. J.; Poe, M. P.; Braegelmann, P. K.; Baldwin, D. W.; Van Way, V. (1976) Ozone dosage-crop loss
10             function for alfalfa: a standardized method for assessing crop losses from air pollutants. J. Air Pollut.
11             Control Assoc. 26: 861-865.
12
13     Oshima, R. J.; Braegelmann, P. K.; Baldwin, D. W.; Van Way, V.; Taylor, O. C. (1977a) Reduction of tomato
14             fruit size and yield by ozone. J. Am. Soc. Hortic. Sci. 102: 289-293.
15
16     Oshima, R. J.; Braegelmann, P. K.; Baldwin, D. W.; Van Way, V.; Taylor, O. C. (1977b) Responses of five
17             cultivars of fresh market tomato to ozone: a contrast of cultivar screening with foliar injury and yield.
18             J. Am. Soc. Hortic.  Sci.  102: 286-289.
19
20     Otto, H. W.; Daines,  R. H.  (1969) Plant injury by air pollutants: influence of humidity on stomatal apertures and
21             plant response to ozone. Science (Washington, DC) 163:  1209-1210.
22
23     Parry, M.  A. J.;  Day,  W. (1988) A comparison of indices that describe the relationship between exposure  to
24             ozone and the reduction in the yield of agricultural crops [Comments on article by Lefohn et al., 1988].
25             Atmos. Environ. 22: 2057-2058.
26
27     Parsons, D. J.; Pitelka, L. F. (1991) Plant ecological genetics and air pollution stress: a commentary on
28             implications for natural populations. In: Taylor, G.  E., Jr.; Pitelka, L. F.;  Clegg, M. T., eds. Ecological
29             genetics and air pollution. New York, NY: Springer-Verlag; pp. 337-343.
30
31     Pathak, S.  N.; Love, D. V.; Roy, D. N. (1986) Determination of a chemical basis of air-pollution stress in wood
32             of mature white pine trees in the susceptive  forest ecosystems. Water Air Soil Pollut. 31: 385-392.
33
34     Patton, R.  L. (1981) Effects of ozone and sulfur dioxide on height and stem specific gravity of Populus hybrids.
35             Washington, DC: USDA Forest Service research  paper;  paper no. NE-471.
36
37     Patton, R.  L.; Jensen,  K. F.; Schier, G. A.  (1991) Responses of red spruce seedlings to ozone and acid
38             deposition. Can. J.  For. Res. 21: 1354-1359.
39
40     Payer, H.  D.; Pfirrmann, T.; Kloos, M.; Blank, L. W. (1990) Clone and soil effects on the growth of young
41             Norway spruce during 14 months exposure to ozone plus acid mist. Environ. Pollut. 64: 209-227.
42
43     Pearce, D. (1993) Economic values and the natural world. Earthscan Publications, Ltd.
44
45     Pearcy, R. W.; Bjorkman, O.; Caldwell, M. M.; Keeley, J. E.;  Monson, R. K.; Strain, B. R. (1987) Carbon
46            gain by plants in natural  environments. Bioscience 37: 21-30.
47
48     Pedersen,  B. S.  (1989) Ozone injury Jeffrey and ponderosa pines surrounding Lake Tahoe, California and
49            Nevada. In: Olson, R. K.; Lefohn, A. S., eds.  Effects of air pollution on western forests. Pittsburgh,
50            PA: Air and Waste Management Association; pp. 279-292 (Transactions series no. 16).
51
52     Pell, E. J. (1976) Influence  of benomyl soil treatment on pinto bean plants exposed to peroxyacetyl nitrate and
53            ozone. Phytopathology 66: 731-733.
54


         December 1993                              5-396       DRAFT-DO NOT QUOTE OR CITE

-------
  1     Pell, E. J. (1988) Secondary metabolism and air pollutants. In: Gaseous air pollution and plant metabolism:
  2            proceedings of the 2nd international symposium; pp. 222-237.
  3
  4     Pell, E. J.; Gardner, W. (1979) Enhancement of peroxyacetyl nitrate injury to petunia foliage by benomyl.
  5            HortScience 14: 61-62.
  6
  7     Pell, E. J.; Pearson, N. S. (1983) Ozone-induced reduction in quantity of ribulose-l,5-bisphosphatecarboxylase
  8            in alfalfa foliage. Plant Physiol. 73: 185-187.
  9
 10     Pell, E. J.; Pearson, N. S. (1984) Ozone-induced reduction in quantity and quality of two potato cultivars.
 11            Environ. Pollut. Ser. A 35: 345-352.
 12
 13     Pell, E. J.; Puente, M. (1986) Emission of ethylene by oat plants treated with ozone and simulated acid rain.
 14            New Phytol. 103: 709-715.
 15
 16     Pell, E. J.; Lukezic, F. L.;  Levine, R. G.; Weisberger, W. C. (1977) Response of soybean foliage to reciprocal
 17            challenges by ozone and a hypersensitive-response-inducing Pseudomonad. Phytopathology
 18            67: 1342-1345.
 19
 20     Pell, E. J.; Pearson, N. S.;  Vinten-Johansen, C. (1988) Qualitative and quantitative effects of ozone and/or sulfur
 21            dioxide on field-grown potato plants. Environ. Pollut.  53: 171-186.
 22
 23     Pell, E. J.; Winner, W. E.; Vinten-Johansen, C.; Mooney, H. A. (1990) Response of radish to  multiple stresses.
 24            I.  Physiological and growth responses to changes in ozone and nitrogen. New Phytol.  115: 439-446.
 25
 26     Pell, E. J.; Eckardt, N.; Enyedi, A. J. (1992) Timing of ozone stress  and resulting status of ribulose
 27            bisphosphate carboxylase/oxygenase and associated net photosynthesis. New  Phytol. 120: 397-405.
 28
 29     Pellisier, M.; Lacasse, N. L.; Cole, H., Jr. (1972) Effectiveness of benzimidazole, benomyl and thiabendazole in
 30            reducing ozone injury to pinto beans. Phytopathology 62: 580-582.
 31
 32     Percy,  K.  E.; Jensen, K. F.; McQuattie, C. J.  (1992) Effects of ozone and acidic  fog on red spruce needle
 33            epicuticular wax production, chemical composition, cuticular membrane ultrastructure and needle
 34            wettability. New Phytol. 122:  71-80.
 35
 36     Perrings, C.; Folke, C.; Maler, K.-G. (1992) The ecology and economics of biodiversity loss: the research
 37            agenda. Ambio 21: 201 -211.
 38
 39     Peterson, D. L.;  Arbaugh, M. J. (1988) An evaluation of the effects of ozone injury on radial growth of
 40            ponderosa pine (Pinus ponderosa) in the southern Sierra Nevada. JAPCA 38: 921-927.
 41
 42     Peterson, D. L.;  Arbaugh, M. J. (1992) Coniferous forests of the Colorado front range. Part B:  ponderosa pine
 43            second-growth stands. In: Olson, R. K.; Binkley, D.; Boehm, M., eds. The response of western forests
 44            to  air pollution. New York, NY: Springer-Verlag; pp.  365 and 385-401. (Billings, W. D.;  Golley, F.;
 45            Lange, O. L.; Olson, J. S.; Remmert, H. Ecological studies; analysis and synthesis v. 97).
 46
 47     Peterson, G. L; Sorg, C. L., eds. (1987) Toward the measurement of total economic value. Washington, DC:
 48            U.S. Department of Agriculture, Rocky Mountain Forest and Range Experiment Station; general
49            technical  report no. RM-148.
50
51      Peterson, D. L.; Arbaugh, M. J.; Wakefield, V. A.;  Miller, P. R. (1987) Evidence  of growth reduction in
52            ozone-injured Jeffrey pine (Pinus jeffreyi Grev. and Balf.) in Sequoia and Kings Canyon  National Parks.
53            JAPCA 37: 906-912.
54


         December 1993                               5.397        DRAFT-DO NOT  QUOTE OR CITE

-------
  1      Peterson, D. L.; Arbaugh,  M. J.; Robinson, L. J. (1989) Ozone injury and growth trends of ponderosa pine in
  2             the Sierra Nevada.  In: Olson, R. K.; Lefohn, A. S., eds. Effects of air pollution on western forests.
  3             Pittsburgh, PA: Air and Waste Management Association; pp. 293-308.
  4
  5      Peterson, D. L.; Arbaugh,  M. J.; Linday, J. R. (1991) Regional growth changes in ozone-stressed ponderosa
  6             pine (Pinus ponderosa) in the Sierra Nevada, California, USA. Holocene 1: 50-61.
  7
  8      Peterson, G. L.; Sorg-Swanson, C.; McCollum, D. W.; Thomas, M. H., eds. (1992) Valuing wildlife resources
  9             in Alaska. Boulder, CO: Westview Press.
10
11      Peterson, D. L.; Silsbee, D. G.; Poth, M.; Arbaugh, M. J.; Biles, F. E. (1993) Growth response of big cone
12             Douglas fir (Pseudotsuga macrocarpa) to long term  ozone exposure in Southern California. Submitted.
13
14      Pezzey, J. (1992) Sustainability: an interdisciplinary guide.  Environ. Values 1: 321-362.
15
16      Pier, P. A.; Thornton, F. C.; McDuffie, C., Jr.;  Hanson, P. J. (1992) CC>2 exchange rates of red spruce during
17             the second season of exposure to ozone and acidic cloud deposition. Environ. Exp. Bot. 32: 115-124.
18
19      Pitcher, L. H.; Brennan, E.; Hurley, A.; Dunsmuir, P.; Tepperman, J. M.; Zilinskas, B.  A. (1991)
20             Overproduction of petunia chloroplastic copper/zinc superoxide dismutase does not confer ozone tolerance
21             in transgenic tobacco. Plant Physiol. 97: 452-455.
22
23      Pitelka, L. F. (1988) Evolutionary responses of plants to anthropogenic pollutants. Trends hi Ecology and
24             Evolution 3:  233-236.
25
26      Pleijel, H.; Skarby, L.; Wallin, G.;  Sellden, G. (1989) Yield and grain quality of spring wheat exposed to ozone
27             in open-top chambers. Commission of the European Communities research report no. 19; pp. 138-146.
28
29      Pleijel, H.; Skarby, L.; Wallin, G.;  Sellden, G. (1991) Yield and grain quality of spring wheat (Triticum
30             aestivum L., cv. Drabant) exposed to different concentrations of ozone in open-top chambers. Environ.
31             Pollut. 69: 151-168.
32
33      Pleijel, H.; Skarby, L.; Ojanpera, K.; Sellden, G. (1992) Yield and quality of spring barley, Hordeum vulgare
34             L., exposed to different concentrations of ozone in  open-top chambers. Agric. Ecosyst. Environ.
35             38: 21-29.
36
37      Poth, M. A.; Fenn, M. E.; Huettl, R. F. (1991) Foliar nutrient responses of ozone-impacted, mature ponderosa
38             pine trees in the San Bernardino Mountains of southern California. Presented at: Tropospheric ozone and
39             the environment II: effects, modeling and control, and  the response of southern commercial forests to air
40             pollution; November; Atlanta, GA. Pittsburgh, PA: Air and Waste Management Association.
41
42      Povilaitis, B. (1967) Gene effects for tolerance to weather fleck hi tobacco. Can. J. Genet. Cytol. 9: 327-334.
43
44      Powles, S. B. (1984) Photoinhibition of photosynthesis induced by visible light.  Annu. Rev. Plant Physiol.
45             35: 15-44.
46
47      Prasad, K.; Weigle,  J. L.;  Sherwood, C. H. (1970) Variation  in ozone phytotoxicity among Phaseolus vulgaris
48             cultivars. Plant Dis. Rep.  54: 1026-1027.
49
50      Price, H.; Treshow,  M. (1972) Effects of ozone on the growth and reproduction of grasses. In: Proceedings of
51             the international air pollution conference; Melbourne, Australia. Melbourne, Australia: Clean Air Society
52             of Australia and New Zealand; pp. 275-280.
53
         December 1993                               5-398       DRAFT-DO NOT QUOTE OR CITE

-------
  1      Price, A.; Lucas, P. W.; Lea, P. J. (1990) Age dependent damage and glutathione metabolism in ozone
  2             fumigated barley: a leaf section approach. J. Exp. Bot. 41: 1309-1317.
  3
  4      Prokipcak, B.; Ormrod, D. P. (1986) Visible injury and growth responses of tomato and soybean to combinations
  5             of nickel, copper and ozone. Water Air Soil Pollut. 27: 329-340.
  6
  7      Pronos, J.; Vogler, D. R.; Smith, R. S. (1978) An evaluation of ozone injury to pines in the southern Sierra
  8             Nevada. San Francisco: USDA Forest Service; forest pet management report no. 78-1.
  9
10      Pye, J. M. (1988) Impact of ozone on the growth and yield of trees: a review. J. Environ. Qual. 17: 347-360.
11
12      Qiu, Z.; Chappelka, A. H.; Somers, G. L.; Lockaby, B. G.; Meldahl, R. S. (1992) Effects of ozone and
13             simulated acidic precipitation on above- and below-ground growth of loblolly pine (Pinus taeda). Can.
14             J. For.  Res. 22: 582-587.
15
16      Queiroz, O. (1988) Air pollution, gene expression and post-translational enzyme modifications.
17             In: Schulte-Hostede, S.; Darrall, N. M.; Blank, L. W.; Wellburn, A. R., eds. Air pollution and plant
18             metabolism. London, United Kingdom: Elsevier Applied Science; pp. 238-254.
19
20      Rafarel, C. R.; Ashenden, T. W. (1991) A facility for the large-scale exposure of plants to gaseous atmospheric
21             pollutants. New Phytol. 117: 345-349.
22
23      Rajput, C. B. S.; Ormrod, D. P. (1976) Response of eggplant  cultivars to ozone. HortScience 11: 462-463.
24
25      Randall, A. (1988)  What mainstream economists have to say about the value of biodiversity. In: Wilson, E. O.,
26             ed. Biodiversity. Washington, DC: National Academy Press.
27
28      Randall, A. (1991a) The value of biodiversity. Ambio 20: 64-68.
29
30      Randall, A. (1991b) Total and nonuse values. In:  Braden, J.  B.; Kolstad, C. D., eds. Measuring the demand for
31             environmental quality. New York, NY: Elsevier Science Publishers.
32
33      Rawlings, J. O.; Cure, W. W. (1985) The Weibull function as a dose-response model to describe ozone effects
34             on crop yields. Crop Sci. 25: 807-814.
35
36      Rawlings, J. O.; Lesser, V. M.; Dassel, K.  A. (1988a) Statistical approaches to assessing crop loss. In: Heck,
37             W. W.; Taylor, O. C.; Tingey, D. T., eds. Assessment of crop loss from atmospheric pollutants. New
38             York, NY:  Elsevier Science; pp. 389-416.
39
40      Rawlings, J. O.; Lesser, V. M.; Heagle, A. S.; Heck, W. W.  (1988b) Alternative ozone dose metrics to
41             characterize ozone impact on crop yield loss. J. Environ. Qual. 17: 285-291.
42
43      Rawlings, J. O.; Barrows, C. F.; Flagler, R. B. (1993) Combined analyses of three southern species exposed to
44             ozone and acidic rain: I. statistical analyses. J. Environ. Qual.: submitted.
45
46      Razumovskii, S. D.; Batashova, L. S. (1970) Mechanism of protection against ozone by
47             N-phenyl-N'-isopropyl-p-phenylenediamine. Rubber Chem. Technol. 43: 1340-1348.
48
49      Razumovskii, S. D.; Podmasteriev, V. V.; Zaikov, G. E. (1988) Kinetics and mechanism of stress relaxation of
50             polyisoprene vulcanizates under ozone ageing. Polym. Degrad. Stab. 20: 37-47.
51
52      Rebbeck, J.; Brennan, E. (1984) The effect of simulated acid rain and ozone on the yield and quality of
53             glasshouse-grown alfalfa. Environ. Pollut. Ser. A 36: 7-16.
54


         December 1993                               5.399       DRAFT-DO  NOT QUOTE OR CITE

-------
  1      Rebbeck, J.; Blum, U.; Heagle, A. S. (1988) Effects of ozone on the regrowth and energy reserves of a ladino
  2             clover-tall fescue pasture. J. Appl. Ecol. 25: 659-682.
  3
  4      Rebbeck, J.; Jensen, K. F.; Greenwood, M. S.  (1992) Ozone effects on the growth of grafted mature and
  5             juvenile red spruce. Can. J.  For. Res. 22: 756-760.
  6
  7      Reddy, G.  B.; Reinert, R. A.; Eason, G. (1991a) Effect of acid rain and ozone on soil and secondary needle
  8             nutrients of loblolly pine. In: Wright, R. J.; Baligar, V. C.; Murrmann, R. P., eds. Plant-soil
  9             interactions at low pH: proceedings of the second international symposium; June  1990; Beckley, WV.
10             Dordrecht, The Netherlands: Kluwer Academic Publishers; pp. 139-145.
11
12      Reddy, G.  B.; Reinert, R. A.; Eason, G. (1991b) Enzymatic changes in the rhizosphere of loblolly pine exposed
13             to ozone and acid rain. Soil Biol. Biochem. 23: 1115-1119.
14
15      Reich, P. B. (1987) Quantifying plant response  to ozone: a unifying theory. Tree Physiol. 3:  63-91.
16
17      Reich, P. B.; Amundson, R. G. (1985) Ambient levels of ozone reduce net photosynthesis in tree and crop
18             species. Science (Washington, DC) 230: 566-570.
19
20      Reich, P. B.; Schoettle, A. W.; Stroo, H. F.; Troiano, J.; Amundson, R. G. (1985) Effects of 03, SO2, and
21             acidic rain on mycorrhizal infection in northern red oak seedlings. Can. J. Bot. 63: 2049-2055.
22
23      Reich, P. B.; Schoettle, A. W.; Stroo, H. F.; Amundson, R. G. (1986a) Acid rain and ozone influence
24             mycorrhizal infection  in tree seedlings. J. Air Pollut. Control Assoc. 36:  724-726.
25
26      Reich, P. B.; Schoettle, A. W.; Amundson, R.  G.  (1986b) Effects of Gj and acidic rain  on photosynthesis and
27             growth in sugar maple and northern red oak seedlings. Environ. Pollut. Ser.  A 40: 1-15.
28
29      Reich, P. B.; Schoettle, A. W.; Stroo, H. F.; Troiano, J.; Amundson, R. G. (1987) Effects of ozone and acid
30             rain on white pine (Pinus strobus) seedlings grown in five soils. I. Net photosynthesis and growth. Can.
31             J. Bot. 65: 977-987.
32
33      Reich, P. B.; Shoettle, A. W.; Stroo, H. F.; Amundson, R. G.  (1988) Effects of ozone and acid  rain on white
34             pine (Pinus strobus) seedlings grown in five soils. HI. Nutrient relations. Can. J. Bot. 66:  1517-1531.
35
36      Reich, P. B.; Ellsworth, D. S.; Kloeppel, B. D.; Fownes, J. H.; Gower, S.  T. (1990) Vertical variation in
37             canopy structure and CC>2 exchange in oak-maple forests: influence of ozone, nitrogen, and other factors
38             on  simulated canopy carbon gain. Tree Physiol. 7: 329-345.
39
40      Reiling, K.; Davison, A. W.  (1992a) Spatial variation in ozone resistance of British populations of Plantago
41             major L.  New Phytol. 122: 699-708.
42
43      Reiling, K.; Davison, A. W.  (1992b) The response of native, herbaceous species to ozone: growth and
44             fluorescence screening. New Phytol. 120: 29-37.
45
46      Reiling, K.; Davison, A. W.  (1992c) Effects of a short ozone exposure given at different stages in the
47             development of Plantago major L. New Phytol. 121: 643-347.
48
49      Reinert, R. A. (1984) Plant response to air pollutant mixtures. Ann. Rev. Phytopathol. 22: 421-442.
50
51      Reinert, R. A.; Gooding, G.  V., Jr. (1978) Effect of ozone and tobacco streak virus alone and in combination on
52             Nicotiana tabacum. Phytopathology 68: 15-17.
53
         December 1993                               5-400       DRAFT-DO NOT QUOTE OR CITE

-------
  1     Reinert, R. A.; Gray, T. N. (1981) The response of radish to nitrogen dioxide, sulfur dioxide, and ozone, alone
  2            and in combination. J. Environ. Qual. 10: 240-243.
  3
  4     Reinert, R. A.; Henderson, W. R. (1980) Foliar injury and growth of tomato cultivars as influenced by ozone
  5            dose and plant age. J.  Am. Soc. Hortic. Sci. 105: 322-324.
  6
  7     Reinert, R. A.; Nelson, P. V. (1979) Sensitivity and growth of twelve Elatior begonia cultivars to ozone.
  8            HortScience 14: 747-748.
  9
 10     Reinert, R. A.; Nelson, P. V. (1980) Sensitivity and growth of five Elatior begonia cultivars to SC^ and O3,
 11            alone and in combination. J.  Am. Soc. Hortic. Sci. 105: 721-723.
 12
 13     Reinert, R. A.; Tingey, D. T.; Carter,  H. B. (1972) Sensitivity of tomato cultivars to ozone 1,3. J. Am. Soc.
 14            Hortic. Sci. 97: 149-151.
 15
 16     Reinert, R. A.; Heggestad, H. E.; Heck,  W. W. (1982) Response and genetic modification of plants for
 17            tolerance to air pollutants. In: Christiansen, M. L.; Lewis, C. F., eds. Breeding plants for less favorable
 18            environments. New York, NY:  John Wiley and Sons; pp. 259-292.
 19
 20     Reinert, R. A.; Dunning, J. A.; Heck,  W. W.; Benepal,  P. S.; Rangappa, M. (1984) Screening of bean
 21            (Phaseolus vulgaris) for sensitivity to ozone. HortScience 19: 86-88.
 22
 23     Reinert, R. A.; Rufty, R.  C.; Eason, G. (1988)  Interaction of tobacco etch or tobacco vein mottling virus and
 24            ozone on biomass changes in burley tobacco. Environ.  Pollut. 53: 209-218.
 25
 26     Reinert, R.; Sanchez, B.; Salleras, J. M.; Bermejo, V.; Ochoa, M. J.; Tarruel, A. (1992) Ozone effects on
 27            watermelon plants at the Ebro Delta (Spain): symptomatology. Agric. Ecosyst. Environ. 38: 41-49.
 28
 29     Renaud, J.-P.; Allard, G.; Mauffette, Y. (1992) Differential effects of ozone on two alfalfa cultivars. Plant
 30            Physiol. 99(suppl. 1): 41.
 31
 32     Resh, H. M.; Runeckles, V. C. (1973)  Effects of ozone on bean rust Uromyces phaseoli. Can. J. Bot.
 33            51: 725-727.
 34
 35     Retzlaff, W. A.; Williams, L.  E.; DeJong, T. M. (1991)  The effect  of different atmospheric ozone partial
 36            pressures on photosynthesis and growth of nine fruit and nut tree species. Tree Physiol. 8: 93-105
 37
 38     Retzlaff, W. A.; DeJong, T. M.; Williams,  L. E. (1992a) Photosynthesis and growth response of almond to
 39            increased atmospheric ozone partial pressures. J. Environ. Qual. 21: 208-216.
 40
 41     Retzlaff, W. A.; Williams, L.  E.; Dejong, T. M. (1992b) Photosynthesis growth and yield response of
 42            Casselman plum to various ozone partial pressures during orchard establishment. J. Am. Soc. Hortic.
 43            Sci. 117: 703-710.
 44
 45     Rich, S.; Turner, N. C. (1972) Importance of moisture on stomatal behavior of plants subjected to ozone. J. Air
 46            Pollut. Control Assoc.  22: 718-721.
 47
 48     Rich, S.; Waggoner, P. E.; Tomlinson, H. (1970) Ozone  uptake by bean leaves. Science (Washington, D.C.)
 49            169: 79-80.
 50
51      Richards, B. N. (1987) The microbiology of terrestrial ecosystems. Essex, United Kingdom: Longman Scientific
52             and Technical.
53
         December 1993                               5.491       DRAFT-DO NOT QUOTE OR CITE

-------
  1     Richards, B.  L.; Middleton, J. T.; Hewitt, W. B. (1958) Air pollution with relation to agronomic crops:
  2             V. oxidant stipple of grape. Agron. J. 50: 559-561.
  3
  4     Roberts, B. R. (1990) Physiological response of yellow-poplar seedlings to simulated acid rain, ozone fumigation
  5             and drought. For. Ecol. Manage. 31: 215-224.
  6
  7     Roberts, B. R.; Cannon, W. N., Jr. (1992) Growth and water relationships of red spruce seedlings exposed to
  8             atmospheric deposition and drought. Can. J. For. Res. 22: 193-197.
  9
10     Rodecap, K.  D.; Tingey, D. T. (1986) Ozone-induced ethylene release from leaf surfaces. Plant  Sci. 44: 73-76.
11
12     Rogers, H. H.; Bingham, G. E.; Cure, J. D.; Smith, J. M.; Surano, K. A. (1983) Responses of selected plant
13             species to elevated carbon dioxide in the  field. J. Environ. Qual. 12: 569-574.
14
15     Rolston, H, III. (1988) Environmental ethics: duties to and values in the natural world. Philadelphia, PA: Temple
16             University Press.
17
18     Roose, M. L. (1991) Genetics of response to atmospheric pollutants. In: Taylor, G. E., Jr.; Pitelka, L. F.;
19             Clegg, M. T., eds.  Ecological genetics and air pollution. New York, NY: Springer-Verlag; pp. 111-126.
20
21     Roose, M. L.; Bradshaw, A.  D.; Roberts, T. M. (1982) Evolution of resistance to gaseous air pollutants.
22             In: Unsworth, M. H.; Ormrod, D.  P., eds. Effects of gaseous air pollution in agriculture and
23             horticulture. London, United Kingdom: Butterworth Scientific; pp. 379-409.
24
25     Rosen, P. M.; Runeckles, V. C. (1976) Interaction of ozone and greenhouse whitefly in plant injury. Environ.
26             Conserv.  3: 70-71.
27
28     Rosenthal, D. H.; Nelson, R. H. (1992) Why existence values should not be used in cost-benefit analysis.
29             J. Policy  Anal. Manage. 11: 116-122.
30
31     Rubin, J.; Helfand, G.; Loomis, J. (1991)  A benefit-cost analysis of the northern spotted owl: results from a
32             contingent valuation survey. J. For. 89(12): 25-30.
33
34     Runeckles, V. C. (1974) Dosage of air pollutants and damage to vegetation. Environ. Conserv. 1: 305-308.
35
36     Runeckles, V. C. (1984) Impact of air pollutant combinations on plants. In: Treshow, M., ed. Air pollution and
37             plant life. New York, NY: John Wiley & Sons;  pp. 239-258. (Polunin, N., ed. Environmental
38             monographs and symposia).
39
40     Runeckles, V. C. (1988) A comparison of indices that describe the relationship between exposure to ozone and
41             reduction in the yield of agricultural crops [Comments on article by Lefohn et al., 1988]. Atmos.
42             Environ.  22: 1241-1242.
43
44     Runeckles, V. C. (1992) Uptake of ozone by vegetation. In: Lefohn, A. S., ed. Surface-level ozone exposures
45             and their effects on vegetation. Chelsea, MI: Lewis Publishers, Inc.; pp.  157-188.
46
47     Runeckles, V. C.; Chevone,  B. I. (1992) Crop responses to ozone. In: Lefohn, A. S., ed. Surface level ozone
48            exposures and their effects on vegetation.  Boca Raton, FL: CRC Press; pp. 185-266.
49
50     Runeckles, V. C.; Krupa, S. V. (1993) The impact of UV-B radiation and ozone on terrestrial vegetation.
51            Environ. Pollut.: in press.
52
53     Runeckles, V. C.; Palmer, K. (1987) Pretreatment with nitrogen dioxide modifies plant response to ozone.
54             Atmos. Environ. 21: 717-719.


         December 1993                               5-402       DRAFT-DO NOT QUOTE OR CITE

-------
  1     Runeckles, V. C.; Wright, E.  F. (1989) Exposure-yield response models for crops. In: Proceedings of the 82nd
  2            annual meeting of the  Air and Waste Management Association; June; Anaheim, CA. Pittsburgh, PA: Air
  3            and Waste Management Association; 89-89.5.
  4
  5     Runeckles, V. C.; Wright, E.  F.; White, D. (1990) A chamberless field exposure system for determining the
  6            effects of gaseous air pollutants on crop growth and yield. Environ. Pollut. 63: 61-77.
  7
  8     Russell, C. S. (1993) Old lessons and new contexts in economic-ecological modeling. In: Milon, J. W.;  Shogren,
  9            J.; Young, M., eds. Integrating economic and ecological indicators: proceedings of the symposium of the
 10            Resource Policy Consortium; May; Washington, DC.
 11
 12     Sagoff, M. (1988) Economy of the earth: philosophy, law and the environment. Cambridge, MA: Cambridge
 13            University Press.
 14
 15     Salmon, R. L. (1970) Systems analysis of the effects of air pollution on materials. Raleigh, NC: National Air
 16            Pollution Control Administration, Economic Effects Research Division; report no. APTD-0943. Available
 17            from: NT1S; Springfield, VA; PB-209192.
 18
 19     Salvin, V. S. (1969) Ozone fading of dyes. Text. Chem. Color. 1: 245-251.
 20
 21     Salvin, V. S. (1970) Textile pollution loss is in the billions. Raleigh News and  Observer (March 28): 4,  p. 10.
 22
 23     Salvin, V. S.; Walker, R. A. (1955) Service fading of disperse dyestuffs by chemical agents other than the oxides
 24            of nitrogen. Text. Res. J. 25: 571-582.
 25
 26     Samuelson, L. J.; Edwards, G. S. (1993) Tree versus seedling sensitivity to ozone in Quercus  rubra L. New
 27            Phytol.: in press.
 28
 29     Sanders, J. S.; Reinert, R. A.  (1982) Screening azalea cultivars for sensitivity to nitrogen dioxide, sulfur dioxide,
 30            and ozone alone and in mixtures. J. Am. Soc. Hortic. Sci. 107: 87-90.
 31
 32     Sanders, G. E.;  Turnbull, N. D.; Clark, A. G.; Colls, J. J. (1990) The growth and development of Viciafaba L.
 33            in filtered and unfiltered open-top chambers. New Phytol. 116: 67-78.
 34
 35     Sanders, G. E.;  Robinson, A.  D.; Geissler, P. A.; Colls, J. J. (1992) Yield stimulation of a commonly grown
 36            cultivar  of Phaseolus vulgaris L.  at near-ambient ozone concentrations. New Phytol. 122: 63-70.
 37
 38     Sasek, T. W.; Richardson, C.  J.  (1989) Effects of chronic doses of ozone on loblolly pine: photosynthetic
 39            characteristics in  the third growing season. For. Sci. 35: 745-755.
 40
 41     Sasek, T. W.; Richardson, C.  J.;  Fendick, E. A.; Bevington, S. R.; Kress,  L.  W. (1991) Carryover effects of
 42            acid rain and ozone on the physiology of multiple flushes of loblolly pine seedlings. For. Sci.
 43            37: 1078-1098.
 44
 45     Saurer, M.; Fiihrer, J.; Siegenthaler, U. (1991) Influence of ozone on the stable carbon isotope composition,
 46            613C, of leaves and grain of spring wheat (Triticum aestivum L.). Plant Physiol. 97: 313-316.
 47
 48     Schenone, G.; Botteschi,  G.; Fumagalli, I.; Montinaro, F. (1992) Effects of ambient air pollution in open-top
49            chambers on bean (Phaseolus vulgaris L.): I. effects on growth and yield. New Phytol. 122: 689-697.

51      Schier, G. A.; McQuattie, C. J.; Jensen,  K. F. (1990) Effect of ozone and aluminum on pitch  pine (Pinus rigida)
52            seedlings: growth and nutrient relations. Can. J. For. Res. 20: 1714-1719.
53
         December 1993                                5-403        DRAFT-DO NOT QUOTE OR CITE

-------
  1      Schneider, P.; Horn, K.; Lauterbach, R.; Hock, B. (1990) Influence of ozone and acid mist on the contents of
  2             gibberellic acid (GA3) in spruce needles (Picea abies) (L.) Karst. Environ. Pollut. 64: 347-351.
  3
  4      Scholz, F.; Gergorius, H.-R.; Rudin, D., eds. (1989) Genetic effects of air pollutants in forest tree populations:
  5             proceedings of the joint meeting of the  FUFRO working parties. Berlin, Federal Republic of Germany:
  6             Springer-Verlag.
  7
  8      Schulze, E.-D.; Cermak, J.; Matyssek, R.; Penka, M.; Zimmermann, R.; Vasicek, F.; Cries, W.; Kucera,
  9             J. (1985) Canopy transpiration and water fluxes in the xylem of the trunk of Larix and Picea
10             trees—a comparison of xylem flow, porometer and cuvette measurements. Oecologia 66: 475-483.
11
12      Scotto, J.; Cotton, G.; Urbach,  F.; Berger, D.; Fears, T. (1988) Biologically effective ultraviolet radiation:
13             surface measurements in the United States, 1974 to 1985. Science (Washington, DC) 239: 762-764.
14
15      Searcy, K. B.; Mulcahey, D.  L. (1985) The parallel expression of metal tolerance in pollen and sporophytes of
16             Silene dioica (L.) Clairv., S. alba (Mill.) Krause and Mimulus guttatus DC. Theor. Appl. Genet.
17             69: 579-602.
18
19      Segerson, K. (1991) Air pollution and agriculture:  a review and evaluation of policy interactions. In: Just, R. E.;
20             Bockstael, N., eds. Commodity and resource policies in agricultural systems. Berlin, Germany:
21             Springer-Verlag;  pp. 349-367.
22
23      Seiler, J.  R.; Cazell, G. H. (1990) Influence of water stress on the physiology and growth of red spruce
24             seedlings. Tree Physiol. 6: 69-77.
25
26      Semeniuk, P.; Heggestad, H.  E. (1981) Differences among Coleus cultivars in tolerance to ozone and sulfur
27             dioxide. J. Hered. 72: 459-460.
28
29      Sen, A. (1987) On ethics and economics.  New  York,  NY: Basil Blackwell Ltd.
30
31      Pearcy, R. W.; Bjorkman, O.; Caldwell,  M.  M.; Keeley, J. E.; Monson, R.  K.; Strain, B. R. (1987) Carbon
32             gain by plants in natural environments.
33
34      Senser, M. (1990) Influence of soil substrate and ozone plus acid mist on the frost resistance of young Norway
35             spruce. Environ. Pollut. 64: 265-278.
36
37      Shafer, S. R. (1988) Influence of ozone and simulated acidic rain on microorganisms in the rhizosphere of
38             sorghum. Environ. Pollut. 51: 131-152.
39
40      Shafer, S. R. (1992) Responses of microbial populations in the rhizosphere to deposition of simulated acidic rain
41             onto foliage and/or soil. Environ. Pollut. 76: 267-278.
42
43      Shafer, S. R.; Heagle, A. S.  (1989) Growth responses of field-grown loblolly pine to chronic doses of ozone
44             during multiple growing seasons.  Can. J. For. Res. 19: 821-831.
45
46      Shafer, S. R.; Schoeneberger, M. M. (1991) Ozone-induced alteration of biomass allocation and nitrogen derived
47             from air in the leguminous plant-Rhizobium-VAM system. In: Keister, D. L.; Cregan, P. B., eds. The
48             rhizosphere and plant growth: papers presented at a symposium; May 1989; Beltsville, MD. Dordrecht,
49             The Netherlands: Kluwer  Academic Publishers; paper no.  377. (Beltsville symposia in agricultural
50             research: no. 14).
51
52      Shafer, S. R.; Heagle, A. S.; Camberato, D. M. (1987) Effects of chronic doses of ozone on field-grown
53             loblolly pine: seedling responses in the  first year. JAPCA 37: 1179-1184.
54


         December 1993                               5-404       DRAFT-DO NOT QUOTE OR CITE

-------
 1     Shafer, S. R.; Reinert, R.  A.;  Eason, G.; Spruill, S. E. (1993) Analysis of ozone concentration-biomass
 2             response relationships among open-pollinated families of loblolly pine. Can. J. For. Res. 23: 706-715.
 3
 4     Sharpe, P. J. H.; Spence, R. D.; Rykiel, E. J., Jr. (1989) Diagnosis of sequential ozone effects on carbon
 5             assimilation, translocation and allocation in cottonwood and loblolly pine. New York, NY: National
 6             Council of the Paper Industry for Air and Steam Improvement, Inc.; technical bulletin no. 565.
 7
 8     Shaver, C. L.; Cass, G. R.; Druzik, J.  R.  (1983) Ozone and the deterioration of works  of art. Environ. Sci.
 9             Technol.  17: 748-752.
10
11     Shaw, P. J.  A.; Dighton, J.; Poskitt, J.; McLeod, A. R. (1992) The effects of sulphur dioxide and ozone on the
12             mycorrhizas of Scots pine and Norway spruce in a field fumigation system.  Mycol. Res.  96: 785-791.
13
14     Shelburne, V. B.; Reardon, J. C.; Paynter, V. A. (1993) The effects of acid  rain and ozone on biomass and leaf
15             area parameters of shortleaf pine (Pinus echinata Mill.). Tree Physiol. 12:  163-172.
16
17     Shimizu, H.; Oikawa, T.;  Totsuka, T. (1984) Effects of low concentrations of NO2 and O3 alone and in mixture
18             on the growth of sunflower plants.  Kenkuritsu Kogai Kenkyusho Kenkyu Hokoku 65: 121-136.
19
20     Shortle, J.; Dunn, J.; Phillips, M. (1986) Economic assessment of crop damage  to air pollution:  the role of
21             quality effects. Pennsylvania State University, Department of Agricultural Economics; staff paper
22             no.  118.
23
24     Showman, R. E.  (1991) A comparison of ozone injury to vegetation during moist and drought years. J. Air
25             Waste Manage.  Assoc. 41: 63-64.
26
27     Shriner, D.  S.; Johnson, J. W., Jr. (1987) The effects of acid rain, alone and in combination with gaseous
28             pollutants, on growth and yield of crop plants. In:  Hutchinson, T. C.; Meema, K.  M., eds. Effects of
29             atmospheric pollutants on forests, wetlands and agricultural ecosystems: proceedings of the NATO
30             advanced research workshop; May 1985; Toronto, Canada. Berlin, Germany:  Springer-Verlag;
31             pp.  481-491. (NATO ASI series G: Ecological sciences, v. 16).
32
33     Shriner, D.  S.; Heck, W. W.; McLaughlin, S. B.; Johnson, D. W.; Irving, P. M.; Joslin,  J. D.; Peterson,
34             C. E. (1990) Response of vegetation to atmospheric deposition and air pollution. In: Acidic deposition:
35             state of science and technology; v.  HI. Washington, DC:  National Acid Precipitation Assessment
36             Program.
37
38     Sigal, L. L.; Johnston, J. W., Jr. (1986) Effects of acidic  rain and ozone and nitrogen fixation and
39             photosynthesis in the lichen Lobaria pulmonaria (L.) Hoffm. Environ. Exp. Bot. 26: 59-64.
40
41     Sigal, L. L.; Suter, G. W., II. (1987) Evaluation of methods for determining adverse impacts of air pollution on
42             terrestrial ecosystems.  Environ. Manage. 11: 675-694.
43
44     Simini, M.; Snyder, R.  G.; Simon, J. E. (1987) Differential sensitivity of muskmelon and watermelon cultivars
45             to ozone-induced foliar injury. Indiana Acad. Sci. 96: 121-127.
46
47     Simini, M.; Skelly, J. M.; Davis, D. D.; Savage, J.  E.; Comrie,  A. C. (1992) Sensitivity of four hardwood
48             species to ambient ozone in north central Pennsylvania. Can. J.  For. Res. 22: 1789-1799.
49
50     Simmons, G.  L.; Kelly, J. M. (1989) Influence of O3, rainfall acidity, and soil Mg status on growth and
51             ectomycorrhizal colonization of loblolly pine roots. Water Air Soil Pollut. 44: 159-171.
52
53     Skarby, L.;  Troeng, E.; Bostrom, C.-A. (1987) Ozone uptake and effects on transpiration,  net photosynthesis,
54             and dark respiration in Scots pine.  For. Sci. 33: 801-808.


         December 1993                               5-405       DRAFT-DO NOT  QUOTE OR CITE

-------
  1     Skelly, J. M. (1980) Photochemical oxidant impact on Mediterranean and temperate forest ecosystems: real and
  2            potential effects. In: Miller, P. R., ed. Proceedings of symposium on effects of air pollutants on
  3            Mediterranean and temperate forest ecosystems; June; Riverside, CA. Berkeley, CA: U.S. Department of
  4            Agriculture,  Forest Service; pp. 38-50; report no. PSW-43. Available from: NITS, Springfield, VA;
  5            PB81-133720.
  6
  7     Skelly, J. M. (1989) Forest decline versus tree decline—the pathological considerations. Environ. Monit. Assess
  8            12: 23-27.
  9
10     Skelly, J. M.; Croghan, C. F.; Hayes, E. M. (1977) Oxidant levels in remote mountainous areas of southwestern
11            Virginia and their effects on native white pine (Pinus strobus L.). In: Dimitriades, B., ed. International
12            conference on photochemical oxidant pollution and its control—proceedings: v. II; September 1976;
13            Raleigh, NC. Research Triangle Park,  NC: U.S. Environmental Protection Agency,  Environmental
14            Sciences Research  Laboratory; pp. 611-620; EPA report no. EPA-600/3-77-001b. Available from:  NTIS,
15            Springfield, VA; PB-264233.
16
17     Slaughter, L. H.; Mulchi,  C. L.; Lee,  E. H.; Tuthill, K. (1989) Chronic ozone stress effects on yield and  grain
18            quality of soft red winter wheat. Crop Sci. 29: 1251-1255.
19
20     Smith, V. K. (1989) Taking stock hi progress with travel cost recreation demand methods: theory and
21            implementation. Mar. Resour. Econ. 6: 279-310.
22
23     Smith, V. K. (1993) Nonmarket values for environmental resources: an interpretive appraisal. Land Econ.
24            69: 1-26.
25
26     Smith, W. H.  (1992) Air pollution effects on ecosystem processes. In: Barker, J. R.; Tingey, D. T., eds. Air
27            pollution effects on biodiversity. New York, NY:  Van Nostrand Reinhold; pp.  234-260.
28
29     Smith, G.; Greenhalgh, B.; Brennan, E.; Justin, J. (1987) Soybean yield in New Jersey relative to ozone
30            pollution and antioxidant application. Plant Dis. 71: 121-125.
31
32     Smith, G.; Neyra, C.; Brennan, E. (1990) The relationship between foliar injury, nitrogen metabolism, and
33            growth parameters in ozonated soybeans. Environ. Pollut. 63: 79-93.
34
35     Snyder, R. G.; Simon, J. E.; Reinert, R. A.; Simini, M.; Wilcox, G. E. (1991) Effects of air quality on growth
36            yield and quality of watermelon. Hortscience 26: 1045-1047.
37
38     Somerville, M. C.; Shadwick, D. S.;  Meldahl, R. S.; Chappelka, A. H.; Lockaby, B.  G. (1992) Use of a
39            non-linear model in examining growth responses of loblolly pine to ozone and acid precipitation. Atmos.
40            Environ. Part A 26: 279-286.
41
42     Spence, J. W.; Haynie, F. H. (1972) Paint technology and air pollution: a survey and economic assessment.
43            Research Triangle  Park, NC: U.S.  Environmental Protection Agency, Office of Air Programs;
44            publication no. AP-103. Available from: NTIS, Springfield, VA; PB-210736.
45
46     Spence, R. D.; Rykiel, E.  J., Jr.; Sharpe, P. J. H. (1990) Ozone alters carbon allocation hi loblolly pine:
47            assessment with carbon-11 labeling. Environ. Pollut.  64: 93-106.
48
49     Stan, H.-J.; Schicker, S.; Kassner, H.  (1981) Stress ethylene evolution of bean plants—a parameter indicating
50            ozone pollution. Atmos. Environ.  15: 391-395.
51
52     Stark, R. W.;  Cobb, F. W., Jr. (1969) Smog injury, root diseases and bark beetle damage in ponderosa pine.
53            Calif.  Agric. 23(9): 13-15.
54


         December  1993                               5-406       DRAFT-DO NOT QUOTE OR CITE

-------
  1      Stasiuk, W. N., Jr.; Coffey, P. E.  (1974) Rural and urban ozone relationships in New York State. J. Air Pollut.
  2             Control Assoc. 24: 564-568.
  3
  4      Steiner, K. C.; Davis, D.  D.  (1979) Variation among Fraxinus families in foliar response to ozone. Can. J. For.
  5             Res. 9: 106-109.
  6
  7      Stevens, T. H.; Echeverria, J.; Glass, R. J.; Hager, T. (1991a) Measuring the existence value of wildlife: what
  8             do CVM estimates really show? Land Econ. 67: 390-400.
  9
10      Stevens, T. H.; Glass, R.; More, T.; Echeverria, J. (1991b) Wildlife recovery: is benefit-cost analysis
11             appropriate? J. Environ. Manage. 33: 327-334.
12
13      Stolte, K. W.;  Duriscoe, D. M.; Cook, E. R.;  Cline, S. P. (1992) Methods of assessing responses of trees,
14             stands and ecosystems to air pollution. In: Olson, R. K.; Binkley, D.; Bohtn, M, eds. The responses of
15             western forests to air  pollution. New York, NY: Springer Verlag; pp. 259-330.
16
17      Stow, T. K.: Allen, H. L.; Kress,  L. W. (1992) Ozone impacts on seasonal foliage dynamics of young loblolly
18             pine. For.  Sci.  38:  102-119.
19
20      Stroo, H.  F.; Reich, P. B.; Schoettle, A. W.; Amundson, R. G. (1988) Effects of ozone and acid rain on white
21             pine (Pinus strobus) seedlings grown in five soils. II. Mycorrhizal infection. Can. J. Bot. 66:  1510-1516.
22
23      Sumizono, T.;  Inoue, T. (1986) Responses of foliar gas exchanges of poplar clones in relation to  resistance to
24             ozone.  Bull. For. For. Prod.  Res. Inst.  (Jpn) 33:  35-44.
25
26      Suter, G.  W., II. (1990) Endpoints for regional ecological risk assessments. Environ. Manage.  14: 9-23.
27
28      Sutton,  R.; Ting, I. P.  (1977) Evidence for the repair of ozone-induced membrane injury. Am. J. Bot.
29             64: 404-411.
30
31      Takemoto, B.  K.;  Shriner, D. S.; Johnston, J. W., Jr. (1987) Physiological responses of soybean (Glycine max
32             L. Merr) to simulated acid  rain and ambient ozone in the field. Water Air Soil Pollut. 33: 373-384.
33
34      Takemoto, B.  K.;  Bytnerowicz, A.; Olszyk, D. M.  (1988a) Depression of photosynthesis growth and yield in
35             field-grown green pepper (Capsicum annuum L.)  exposed to acidic fog and ambient ozone. Plant Physiol.
36             88: 477-482.
37
38      Takemoto, B.  K.;  Hutton, W. J.; Olszyk, D. M. (1988b) Responses of field-grown Medicago saliva L. to acidic
39             fog and ambient ozone. Environ. Pollut. 54: 97-107.
40
41      Takemoto, B.  K.;  Olszyk, D. M.; Johnson, A.  G.; Parada, C.  R. (1988c) Yield responses of field-gown crops to
42             acidic fog  and ambient ozone. J.  Environ. Qual. 17:  192-197.
43
44      Takemoto, B.  K.;  Bytnerowicz, A.; Olszyk, D. M. (1989) Physiological responses of field-grown strawberry
45             (Fragaria x ananassa Duch.) exposed to acidic fog and ambient ozone.  Environ. Exp. Bot. 29: 379-386.
46
47      Taylor,  G. E.  (1993) Role of genotype in the response of loblolly pine (Pinus taeda L.) to tropospheric ozone:
48             effects  at the whole-tree, stand and regional  level. J.  Environ. Qual.: in press.
49
50      Taylor,  G.; Davies, W. J.  (1990) Root growth of Fagus sylvatica: impact of air quality and drought at a site in
51             southern Britain. New Phytol. 116: 457-464.
52
53      Taylor,  G. E.,  Jr.; Hanson, P. J. (1992) Forest trees and tropospheric ozone: role of canopy deposition and leaf
54             uptake in developing exposure-response relationships. Agric. Ecosyst. Environ. 42: 255-273.


         December 1993                               5-407      DRAFT-DO NOT QUOTE  OR CITE

-------
  1     Taylor, O. C.; MacLean, D. C. (1970) Nitrogen oxides and the peroxyacyl nitrates. In: Jacobson, J. S.; Hill,
  2            A. C., eds. Recognition of air pollution injury to vegetation: a pictorial atlas.  Pittsburgh, PA: Air
  3            Pollution Control Association; pp. El-El 4.
  4
  5     Taylor, G. E., Jr.; Norby, R. J. (1985) The significance of elevated levels of ozone on natural ecosystems of
  6            North America. In:  Lee, S. D., ed. Evaluation of the scientific basis for ozone/oxidants standards:
  7            proceedings of an APCA international specialty conference; November 1984; Houston, TX.  Pittsburgh,
  8            PA:  Air Pollution Control  Association; pp. 152-175. (APCA transactions: TR-4).

10     Taylor, G. E., Jr.; Pitelka,  L. F. (1992) Genetic diversity of plant populations and the role of air pollution.
11            In: Barker, J. R.; Tingey,  D. T., eds. Air pollution effects on biodiversity.  New York,  NY: Van
12            Nostrand Reinhold;  pp. 111-130.
13
14     Taylor, O. C.; Stephens, E. R.; Darley, E. F.; Cardiff,  E. A. (1960) Effect of air-borne oxidants on leaves of
15            pinto bean and petunia. J.  Am. Soc. Hortic. Sci. 75: 435-444.
16
17     Taylor, G. E., Jr.; McLaughlin, S. B.; Shriner, D. S. (1982) Effective pollutant dose. In:  Unsworth, M.  H.;
18            Ormrod,  D. P., eds. Effects of gaseous air pollution in agriculture and horticulture. London, United
19            Kingdom: Butterworth Scientific; pp. 458-460.
20
21     Taylor, G. E., Jr.; Norby, R. J.; McLauglin, S. B.; Johnson, A. H.; Turner, R. S. (1986) Carbon dioxide
22            assimilation and growth of red spruce (Picea rubens  Sarg.) seedlings in response to ozone, precipitation
23            chemistry, and soil type. Oecologia (Berlin) 70:  163-171.
24
25     Taylor, G. E., Jr.; Hanson,  P. J.;  Baldocchi, D.  D. (1988a) Pollutant deposition to  individual leaves and  plant
26            canopies: sites of regulation and relationship to injury. In:  Heck,  W. W.; Taylor, O. C.; Tingey,  D. T.,
27            eds.  Assessment of crop loss from air pollutants. New York, NY: Elsevier Applied Science; pp. 227-257.
28
29     Taylor, G. E., Jr.; Ross-Todd, B.  M.; Gunderson, C. A. (1988b) Action of ozone on foliar gas exchange in
30            Glycine max L. Merr: a potential role for endogenous stress ethylene. New Phytol. 110: 301-307.
31
32     Telewski, F. W.  (1992) Ethylene production by different age class ponderosa and Jeffery pine needles as  related
33            to ozone exposure and visible injury. Trees 6:  195-198.
34
35     Temple, P. J. (1988) Injury  and growth of Jeffrey pine and giant sequoia in response to ozone and acidic  mist.
36            Environ.  Exp.  Bot. 28: 323-333.
37
38     Temple, P. J. (1989) Oxidant air pollution effects on plants of Joshua Tree national  monument.  Environ.  Pollut.
39            57: 35-48.
40
41     Temple, P. J. (1990a)  Growth and yield responses of processing tomato (Lycopersicon esculentum Mill.)  cultivars
42            to ozone. Environ. Exp. Bot. 30: 283-291.
43
44     Temple, P. J. (1990b) Growth form and yield responses  of four cotton cultivars to ozone.  Agron. J.
45            82:  1045-1050.
46
47     Temple, P. J. (1991) Variations in responses of dry bean (Phaseolus vulgaris) cultivars to  ozone. Agric. Ecosyst.
48            Environ.  36: 1-11.
49
50     Temple, P. J.; Benoit, L. F. (1988) Effects of ozone and water stress on canopy temperature, water use,  and
51            water use efficiency  of alfalfa. Agron. J.  80: 439-447.
52
53     Temple, P. J.; liiscssar, S. (1979) Response of white bean to bacterial blight, ozone, and antioxidant protection
54            in the field. Phytopathology 69: 101-103.


         December 1993                               5-408      DRAFT-DO NOT QUOTE OR CITE

-------
 1     Temple, P. J.; Taylor, O. C.; Benoit, L. F. (1985) Cotton yield responses to ozone as mediated by soil moisture
 2             and evapotranspiration. J. Environ. Qual. 14: 55-60.
 3
 4     Temple, P. J.; Taylor, O. C.; Benoit, L. F. (1986) Yield response of head lettuce (Lactuca saliva) to ozone.
 5             Environ. Exp. Bot. 26: 53-58.
 6
 7     Temple, P. J.; Lennox, R.  W.; Bytnerowicz, A.; Taylor, O. C. (1987) Interactive effects of simulated acidic fog
 8             and ozone on field-grown alfalfa. Environ. Exp. Bot. 27: 409-417.
 9
10     Temple, P. J.; Benoit, L. F.; Lennox, R. W.; Reagan, C. A.; Taylor, O. C. (1988a) Combined effects of ozone
11             and water stress on alfalfa growth and yield. J. Environ. Qual. 17: 108-113.
12
13     Temple, P. J.; Kupper, R.  S.; Lennox, R. W.; Rohr,  K. (1988b) Injury and yield responses of differentially
14             irrigated cotton to ozone. Agron. J. 80: 751-755.
15
16     Temple, P. J.; Kupper, R.  S.; Lennox, R. L.; Rohr, K. (1988c) Physiological and growth responses of
17             differentially irrigated cotton to ozone. Environ. Pollut. 53: 255-263.
18
19     Temple et al. (1991).
20
21     Temple, P. J.; Riechers, G. H.; Miller, P.  R. (1992) Foliar injury responses of ponderosa pine seedlings to
22             ozone, wet and dry acidic deposition, and drought. Environ. Exp. Bot. 32: 101-113.
23
24     Temple, P. J.; Riechers, G. H.; Miller, P.  R.; Lennox, R. W. (1993) Growth responses of ponderosa pine to
25             long-term exposure to ozone, wet and dry acidic deposition,  and drought. Can. J. For. Res. 23: 59-66.
26
27     Teskey, R. O.; Dougherty, P. M.; Wiselogel, A. E. (1991) Design and performance of branch chambers suitable
28             for long-term ozone fumigation of foliage in large trees. J. Environ. Qual. 20: 591-595.
29
30     Teso, R. R.; Oshima, R. J.; Carmean, M. I. (1979) Ozone-pesticide interactions. Calif. Agric. 33: 13-15.
31
32     Tevini, M.; Teramura, A. H. (1989) UV-B effects on terrestrial plants. Photochem. Photobiol. 50: 479-487.
33
34     Thompson, C. R.; Kats, G.; Pippen,  E. L.; Isom, W. H. (1976) Effect of photochemical air pollution on two
35             varieties of alfalfa.  Environ. Sci. Technol. 10:  1237-1241.
36
37     Thor, E.; Gall, W. B. (1978) Variation in air pollution tolerance and growth rate among progenies of southern
38             Appalachian  white pine. Metria 1: 80-86.
39
40     Thorne,  L.; Hanson, G. P. (1976) Relationship between genetically controlled ozone sensitivity and gas exchange
41             rate in Petunia hybrlda Vilm. J. Am. Soc. Hortic. Sci. 101:  6-63.
42
43     Thornton, F. C.; Pier,  P. A.; McDuffie, C., Jr. (1992) Plant and environment interactions: red spruce response
44             to ozone and cloudwater after three years exposure. J. Environ. Qual. 21: 196-202.
45
46     Tiedemann, A.  V.; Ostlaender, P.; Firsching, F. H.; Fehrmann, H.  (1990) Ozone episodes in southern Lower
47             Saxony (FRG) and  their impact on the susceptibility of cereals to fungal pathogens.  Environ. Pollut.
48             67: 43-59.
49
50     Tiedemann, A.  V.; Weigel, H.-J.; Ja'ger, H.-J. (1991) Effects of open-top chamber fumigations with ozone on
51             three fungal leaf diseases of wheat and the mycoflora of the phyllosphere. Environ.  Pollut. 72: 205-224.
52
53
         December  1993                               5-409       DRAFT-DO NOT QUOTE OR CITE

-------
 1     Tingey, D. T. (1984) The effects of ozone on plants in the United States. In: Grennfelt, P., ed. Proceedings of
 2             the international workshop on the evaluation of the effects of photochemical oxidants on human health,
 3             agricultural crops, forestry, materials and visibility; February-March; Goteborg, Sweden. Goteborg,
 4             Sweden: Swedish Environmental Research Institute; pp. 60-75; report no. IVL-EM 1570.
 5
 6     Tingey, D. T.; Hogsett, W. E. (1985) Water stress reduces ozone injury via a stomatal mechanism. Plant
 7             Physiol. 77: 944-947.
 8
 9     Tingey, D. T.; Taylor, G. E., Jr. (1982) Variation in plant response to ozone: a conceptual model of
10             physiological events. In: Unsworth, M.  H.; Ormrod, D. P., eds. Effects of gaseous air pollution in
11             agriculture and horticulture.  London, United Kingdom: Butterworth Scientific; pp.  113-138.
12
13     Tingey, D. T.; Reinert, R. A.; Carter, H. B. (1972) Soybean cultivars: acute foliar response to ozone. Crop Sci.
14             12: 268-270.
15
16     Tingey, D. T.; Wilhour, R. G.; Standley, C. (1976a) The effect of chronic ozone exposures on the metabolite
17             content of ponderosa pine seedlings. For. Sci. 22: 234-241.
18
19     Tingey, D. T.; Files, R. C.; Wickliff, C. (1976b) Differential foliar sensitivity of soybean cultivars to ozone
20             associated with differential enzyme activities. Physiol. Plant. 37: 69-72.
21
22     Tingey, D. T.; Hogsett, W. E.; Lee, E. H. (1989) Analysis of crop loss for alternative ozone exposure  indices.
23             In: Schneider, T.; Lee, S. D.; Wolters, G. J.  R.; Grant,  L. D., eds. Atmospheric ozone research and its
24             policy implications: proceedings of the 3rd US-Dutch international symposium; May 1988; Nijmegen,
25             The Netherlands. Amsterdam, The Netherlands: Elsevier  Science Publishers; pp. 219-227. (Studies in
26             environmental science 35).
27
28     Tingey, D. T.; Hodsett, W. E.; Henderson, S.  (1990) Definition of adverse effects for the purpose of
29             establishing secondary national ambient air quality standards. J. Environ. Qual. 19:  635-639.
30
31     Tingey, D. T.; Hogsett, W. E.; Lee, E. H.; Herstrom, A. A.; Azevedo, S. H. (1991) An evaluation of various
32             alternative ambient ozone standards based on crop yield loss data. In: Berglund, R.  L.; Lawson, D.  R.;
33             McKee, D. J., eds. Tropospheric ozone and the environment: papers from an  international conference;
34             March 1990; Los Angeles, CA.  Pittsburgh, PA: Air & Waste Management Association; pp. 272-288.
35             (A&WMA transaction series no. TR-19).
36
37     Tingey, D. T.; Olszyk, D. M.; Herstrom, A. A.; Lee, E. H. (1993) Effects of ozone on crops. In: McKee,
38             D. J., ed. Tropospheric ozone:  human health and agricultural impacts. Boca Raton, FL: Lewis
39             Publishers; pp.  175-206.
40
41     Tjoelker, M. G.; Luxmoore,  R. J. (1991) Soil nitrogen and chronic ozone stress influence physiology, growth
42             and nutrient  status of Pinus  taeda L. and Liriodendron tulipifera L.  seedlings. New Phytol. 119: 69-81.
43
44     Todd, A. G.; Ormrod, D. P.; Hale, B. A.; Goodyear, S. N. (1991) Temperature effects on tomato response to
45             ozone at constant vapor pressure deficit. Biotronics 20: 43-52.
46
47     Toivonen, P.  M. A.; Hofstra, G.; Wukasch, R. T. (1982) Assessment of yield losses  in white bean due to ozone
48             using the antioxidant  EDU.  Can. J. Plant Pathol. 4: 381-386.
49
50    Tonneijck, A.  E. G. (1984) Effects  of peroxyacetyl nitrate (PAN) and ozone on some plant species.
51             In: Grennfelt, P., ed. Proceedings of the international workshop on the evaluation of the effects of
52            photochemical oxidants on human health, agricultural crops, forestry, materials and visibility;
53             February-March; Goteborg, Sweden. Goteborg, Sweden: Swedish linvironmnetal Research  Institute;
54            pp. 118-127; report no. IVL-EM 1570.


         December  1993                               5-410       DRAFT-DO NOT QUOTE OR CITE

-------
  1     Torn, M. S.; Degrange, J. E.; Shinn, J. H. (1987) The effects of acidic deposition on Alberta agriculture:
  2             a review (v. 8). Calgary,  AB, Canada: Acid  Deposition Research Program; report no. ADRP-B-08/87.
  3
  4     Townsend, A. M.; Dochinger, L. S. (1974) Relationship of seed source and developmental stage to the ozone
  5             tolerance of Acer rubrum seedlings. Atmos. Environ.  8: 957-964.
  6
  7     Treshow, M. (1980) Pollution effects on plant distribution. Environ. Conserv. 7: 279-286.
  8
  9     Troiano, J.; Colavito, L.; Heller, L.; McCune, D. C.; Jacobson, J. S. (1983) Effects of acidity of simulated rain
10             and its joint action with ambient ozone on measures of biomass and yield in soybean. Environ. Exp. Bot.
11             23: 113-119.
12
13     Trumble, J. T.; Hare, J. D.; Musselman, R. C.;  McCool, P.  M. (1987) Ozone-induced changes hi host-plant
14             suitability: interactions of Keiferia lycopersicella and Lycopersicon esculentum. J. Chem. Ecol.
15             13: 203-218.
16
17     Tseng, E. C.; Seiler, J. R.; Chevone, B. I. (1988) Effects of  ozone and water stress on greenhouse-grown fraser
18             fir seedling growth and physiology. Environ. Exp. Bot. 28: 37-42.
19
20     Turner, N. C.; Rich, S.; Tomlinson, H. (1972) Stomatal conductance, fleck injury, and growth of tobacco
21             cultivars varying in ozone tolerance. Phytopathology 62: 63-67.
22
23     U.S. Environmental Protection Agency. (1978) Air quality criteria for ozone and other photochemical oxidants.
24             Research Triangle Park, NC: Office of Health and Environmental Assessment, Environmental Criteria
25             and Assessment Office; EPA report no. EPA-600/8-78-004. Available from: NTIS, Springfield, VA;
26             PB80-124753.
27
28     U.S. Environmental Protection Agency. (1986) Air quality criteria for ozone and other photochemical oxidants.
29             Research Triangle Park, NC: Office of Health and Environmental Assessment, Environmental Criteria
30             and Assessment Office; EPA report nos. EPA-600/8-84-020aF-eF. 5v. Available from: NTIS,
31             Springfield, VA; PB87-142949.
32
33     U.S. Environmental Protection Agency. (1987) Air pollution exposure systems and experimental protocols.
34             Vol. 2: description of facilities. Corvallis, OR: Corvallis Environmental Research Laboratory; EPA
35             report no. EPA/600/3-87/037b. Available from: NTIS, Springfield, VA; PB88-181698/HSU.
36
37     U.S. Environmental Protection Agency. (1988) Summary of selected new information on effects of ozone on
38             health and vegetation: draft supplement to air quality criteria for ozone and other photochemical oxidants.
39             Research Triangle Park, NC: Office of Health and Environmental Assessment, Environmental Criteria
40             and Assessment Office; EPA report no. EPA-600/8-88-105A. Available from:  NTIS, Springfield, VA;
41             PB89-135123.
42
43     U.S. Environmental Protection Agency. (1989) Review of the national ambient air quality standards for ozone:
44             assessment of scientific and technical information. OAQPS staff paper. Research  Triangle Park, NC:
45             Office of Air Quality Planning  and Standards; EPA report no.  EPA-450/2-92/001. Available from: NTIS,
46             Springfield, VA; PB92-190446.
47
48     U.S. Environmental Protection Agency. (1992a) Summary of  selected new information on effects of ozone on
49             health and vegetation: supplement to 1986 air quality criteria for ozone and other photochemical oxidants.
50             Research Triangle Park,  NC: Office of Health and Environmental Assessment, Environmental Criteria
51             and Assessment Office; EPA report no. EPA/600/8-88/105F. Available from: NTIS, Springfield, VA;
52             PB92-235670.
53
         December 1993                               5.4! i       DRAFT-DO NOT QUOTE OR CITE

-------
  1     U.S. Environmental Protection Agency. (1992b) Framework for ecological risk assessment. Washington, DC:
  2            U.S. Environmental Protection Agency, Risk Assessment Forum; EPA report no. EPA/630/R-92/001.
  3            Available from: NTIS, Springfield, VA; PB93-102192/REB.
  4
  5     U.S. Environmental Protection Agency. (1993) Air quality criteria for oxides of nitrogen. Research Triangle
  6            Park, NC: Office of Health and Environmental Assessment, Environmental Criteria and Assessment
  7            Office; EPA review draft no. EPA/600/8-91/049F.
  8
  9     Umbach, D. M.;  Davis, D. D. (1984) Severity and frequency of SO2-induced leaf necrosis on seedlings of
10            57 tree species. For.  Sci. 30: 587-596.
11
12     Upham, J. B.; Haynie, F. H.; Spence, J.  W. (1976) Fading of selected drapery fabrics by air pollutants. J.  Air
13            Pollut. Control Assoc. 26: 790-792.
14
15     Velissariou, D.; Barnes, J. D.; Davison, A. W. (1992) Has inadvertent selection by plant breeders affected  the
16            O3 sensitivity of modern Greek cultivars of spring wheat? Agric.  Ecosyst. Environ. 38: 79-89.
17
18     Venne, H.; Scholz, F.; Vornweg, A. (1989) Effects of air pollutants on reproductive processes of poplar
19            (Populus spp.) and Scots pine (Pinus sylvestris L.).  In: Scholz, F.; Gregorius, H.-R.; Rudin, D.,  eds.
20            Genetic effects of air pollutants in forest tree populations: proceedings of the joint meeting of the  IUFRO
21            working parties; August  1987; Grosshansdorf, Federal Republic of Germany.  Berlin, Federal Republic of
22            Germany: Springer-Verlag; pp. 89-103.
23
24     Waddell, T. E.  (1974) The economic damages of air pollution. Washington,  DC: U.S. Environmental Protection
25            Agency, Office of Research and Development; EPA report no. EPA-600/5-74-012. Available from:
26            NTIS, Springfield, VA; PB-235701.
27
28     Wallin, G.; Skarby, L.; Sellden, G. (1990) Long-term exposure of Norway spruce Picea abies (L.) Karst.,  to
29            ozone in open-top chambers.  I. Effects on the capacity of net photosynthesis, dark respiration and leaf
30            conductance of shoots of different ages. New Phytol.  115: 335-344.
31
32     Walsh, N. E.; Charlesworth, D. (1992) Evolutionary interpretations of differences in pollen tube growth rates.
33            Q. Rev.  Biol.  67: 19-37.
34
35     Walsh, R. G.; Johnson, D. M.; McKean, J. R. (1992) Benefit transfer of outdoor recreation demand studies,
36            1968-1988. Water Resour. Res. 28: 707-713.
37
38     Wang, D.; Bormann, F. H.;  Karnosky, D. F. (1986a) Regional tree growth  reductions due to ambient ozone:
39            evidence from field experiments. Environ. Sci. Technol. 20: 1122-1125.
40
41     Wang, D.; Karnosky,  D. F.; Bormann, F. H. (1986b) Effects of ambient ozone on the productivity of Populus
42            tremuloides Michx. grown under  field conditions. Can. J. For. Res.  16: 47-55.
43
44     Wang et al. (1991).
45
46     Ward, M. M. (1980) Variation in the response of loblolly pine to ozone [M. Sc. thesis]. Blacksburg, VA:
47            Virginia Polytechnic Institute and State University.
48
49     Waring,  R. H.; Schlesinger,  W. H. (1985) Forest ecosystems: concepts and management. Orlando, FL:
50            Academic Press, Inc.
51
52     Weber, J. A.; Gates, D. M.  (1990) Gas exchange in Quercus rubra (northern red oak) during a drought:  analysis
53            of relations among photosynthesis, transpiration,  and leaf conductance. Tree Physiol. 7: 215-225.
54


         December 1993                               5-412       DRAFT-DO NOT QUOTE OR  CITE

-------
  1      Weber, D. E.; Reinert, R. A.; Barker, K. R. (1979) Ozone and sulfur dioxide effects on reproduction and
  2             host-parasite relationships of selected plant-parasitic nematodes. Phytopathology 69: 624-628.
  3
  4      Weber, J. A.; Plocher, M. D.; Hogsett, W. E. (1991) Effect of ozone exposure on leaf production and retention
  5             in tree seedlings. Bull. Ecol. Soc.  Am. 72: 282-283.
  6
  7      Weber, J. A.; Clark, C. S.; Hogsett, W. E. (1993) Analysis of the relationship among Oj uptake, conductance,
  8             and photosynthesis in needles of Pinusponderosa. Tree Physiol.: in press.
  9
10      Weidmann, P.; Einig, W.; Egger, B.; Hampp, R. (1990) Contents of ATP and ADP in needles of Norway
11             spruce in relation to their development, age, and to symptoms of forest decline. Trees 4: 68-74.
12
13      Weigel, H. J.; Adaros, G.; Jaeger, H. J. (1987)  An open-top chamber study with filtered and non-filtered air to
14             evaluate the effects of air pollutants on crops. Environ. Pollut. 47: 231-244.
15
16      Weinstein, D. A.; Beloin, R.  M.; Yanai, R. D. (1991) Modeling changes in red spruce carbon balance and
17             allocation in response  to interacting ozone and nutrient stress. Tree Phys. 9: 127-146.
18
19      Weir, R. J. (1977) Genetic variation in loblolly pine (Pinus taeda L.) tolerance to ozone [Ph.D. thesis]. Raleigh,
20             NC: North Carolina State University.
21
22      Wenghoefer,  H. M. (1974) Environmental effects on RFL adhesion.  Rubber Chem. Technol. 47: 1066-1073.
23
24      Wesely, M. L.;  Eastman, J. A.; Cook, D.  R.; Hicks,  B. B. (1978) Daytime variations of ozone eddy fluxes to
25             maize. Boundary Layer Meteorol.  15: 361-373.
26
27      Wesely, M. L.;  Eastman, J. A.; Stedman, D. H.; Yalvac, E. D. (1982) An eddy-correlation measurement of
28             NC>2 flux to vegetation and comparison to 03 flux. Atmos. Environ.  16: 815-820.
29
30      Westman, W. E. (1977) How much are nature's  services worth? Measuring the social benefits  of ecosystem
31             functioning is both controversial and illuminating. Science (Washington, DC) 197: 960-964.
32
33      Whitmore, P. M.; Cass, G. R. (1988) The ozone fading of traditional Japanese colorants. Stud. Conserv. 33-40.
34
35      Whitmore, P. M.; Cass, G. R.; Druzik, J.  R. (1987) The ozone fading of traditional natural organic colorants on
36             paper. J. Am. Inst. Conserv. 26: 45-58.
37
38      Whittaker, J. B.; Kristiansen,  L. W.; Mikkelsen, T. N.; Moore, R. (1989) Responses to  ozone of insects feeding
39             on a crop and a weed  species. Environ.  Pollut. 62: 89-101.
40
41      Wieser, G.; Havranek, W. M. (1993) Ozone uptake in the sun and shade crown of spruce:  quantifying the
42             physiological effects of ozone exposure. Trees 7: 227-232.
43
44      Wilton, A. C.;  Murray, J. J.; Heggestad, H. E.; Juska, F. V. (1972) Tolerance and susceptibility of Kentucky
45             bluegrass (Poa pratensis L.) cultivars to air pollution: in the  field and in an ozone chamber.  J. Environ.
46             Qual. 1: 112-114.
47
48      Wiltshire, J. J. J.; Wright, C. J.; Unsworth, M.  H. (1992) A new method for exposing mature trees to ozone
49             episodes. For. Ecol. Manage. 51:  115-120.
50
51      Winner, W. E.;  Atkinson, C.  J. (1986) Absorption of air pollution by plants, and consequences for growth.
52             Trends Ecol. Evol. 1:  15-18.
53
         December 1993                               5-413       DRAFT-DO NOT QUOTE OR CITE

-------
 1     Winner, W. E.; Cotter, I. S.; Powers, H. R., Jr.; Skelly, J. M. (1987) Screening loblolly pine seedling
 2            responses to SO2 and O3: analysis of families differing in resistance to fusiform rust disease. Environ.
 3            Pollut. 47: 205-220.
 4
 5     Wiselogel,  A. E. (1991) Response of loblolly pine seedling genetic variation to ozone. In; Proceedings of the 21st
 6            southern forest tree improvement conference; June; Knoxville, TN. Southern Forest Tree Improvement
 7            Committee; publication no. 43.
 8
 9     Wiselogel,  A. E.; Bailey, J. K.; Newton, R. J.; Fong, F. (1991) Growth response of loblolly pine (Pinus taeda
10            L.) seedlings to ozone fumigation. Environ. Pollut. 71: 43-56.
11
12     Wolfenden, J.; Wellburn, A. R. (1991) Effects of summer ozone on membrane lipid composition during
13            subsequent frost hardening in Norway spruce (Picea albies (L.) Karst.). New Phytol.  118: 323-329.
14
15     Wolfenden, J.; Wookey, P.  A.;  Lucas, P. W.; Mansfield, T. A. (1992) Action of pollutants individually and in
16            combination. Ih: Barker, J. R.; Tingey, D. T., eds.  Air pollution effects on biodiversity. New York,
17            NY: Van Nostrarid Reinhold; pp. 72-92.
18
19     Wolters,  J. H. B.; Martens, M.  J. M. (1987) Effects of air pollutants on pollen. Bot. Rev. 53: 372-414.
20
21     Woodbury, P. B.; Amundson, R. G.; Kohut, R. J.;  Laurence, J. A.  (1991) Stomatal conductance, whole-tree
22            water use, and foliar carbohydrate status of red spruce saplings exposed to ozone, acid precipitation, and
23            drought. In: Berglund, R., ed. Transactions of the 1991 air and waste Management  Association
24            international symposium on tropospheric ozorie and the environment II. Pittsburgh, PA: Air and Waste
25            Management Association; pp. 618-628.
26
27     Woodward, F. I. (1992) Predicting plant responses to global environmental change. New Phytol. 122: 239-251.
28
29     Wukasch, R. T.; Hofstra, G. (1977a) Ozone and Botrytis interactions in onion-leaf dieback: open-top chamber
30            studies. Phytopathology 67:  1080-1084.
31
32     Wukasch, R. T.; Hofstra, G. (1977b) Ozone and Botrytis spp. interaction in onion leaf dieback: field studies.
33            J. Am. Soc. Hortic. Sci. 102: 543-546.
34
35     Yang, Y.-S.; Skelly, J. M,; Chevone, B. I. (1982) Clonal response of eastern white pine to low doses of O3,
36             SO2, and NO2, singly and in combination. Can. J. For. Res. 12: 803-808.
37
38     Yarwood,  C. E.; Middleton, J.  T. (1954) Smog injury and rust infection. Plant Physiol. 29: 393-395.
39
40     Yocom,  J. E.; Grappone, N. (1976) Effects of power plant emissions on materials. Palo Alto, CA: Electric
41             Power Research Institute; report no. EPRI/EC-139. Available from: NTIS, Springfield, VA;  PB-257539.
42
43     Yocom,  J. E.; Kawecki, J.  M.; Hoffnagle, G. F. (1985) Estimating materials damage  from oxidant pollutants.
44            In: Proceedings of the APCA specialty conference: evaluation of the scientific  basis for ozone/oxidants
45             standards; November 1984;  Houston, TX. Pittsburgh, PA: Air Pollution Control Association.
46
47     Yocom,  J. E.; Baer, N. S.; Robinson, E. (1986)  Air pollution effects on physical and  economic systems.
48            In: Stern, A. C., ed. Air pollution, v. VI. New York, NY: Academic Press; pp. 143-246.
49
50
          December 1993                               5-414       DRAFT-DO NOT QUOTE OR CITE

-------
1     Zeiger, E.; Farquhar, G. D.; Cowan, I. R. (1987) Stomatal physiology. Stanford, CA: Stanford University
2            Press.
3
4     Zeronian, S. H.; Alger, K. W.; Omaye, S. T. (1971) Reaction of fabrics made from synthetic fibers to air
5            contaminated with nitrogen dioxide, ozone, or sulfur dioxide. In:  Englund, H. M.; Beery, W. T.,  eds.
6            Proceedings of the second international clean air congress; December 1970;  Washington, DC. New York,
7            NY: Academic Press; pp. 468-476.
8
      December 1993                             5_415      DRAFT-DO NOT QUOTE OR CITE

-------
                              APPENDIX  5A
                    COLLOQUIAL AND LATIN NAMES
Alder
Alfalfa
Ash, green
Ash, white
Aspen
Avocado
Azalea
Barley
Basswood (linden)
Bean, broad
Bean, kidney, pinto, snap, white
Beech,  American
Beech,  European
Begonia
Birch, paper
Cabbage
Celery
Cherry, black
Citrus (lemon)
Clover, ladino, white
Clover, red
Corn
Cotton
Cottonwood (poplar)
Cress, garden
Cucumber
Dock
Geranium
Fescue, tall
Fir, Douglas
Fir, Fraser
Golden-rain
Grape
Honey locust
Ivy
Kenaf
Juniper, shore
Lettuce
Lilac
Mangel
Alnus serrulata (Aiton) Willdenow
Medicago sativa L.
Fraxinus pennsylvanica Marsh.
Fraxinus americana L.
Populus tremuloides L.
Persea americana Mill.
Rhododendron spp.
Hordewn vulgare L.
Tilia americana L.
Viciafaba L.
Phaseolus vulgaris L.
Fagus quadrifolia Ehrh.
Fagus sylvatica L.
Begonia sp.
Betula papyri/era Marsh
Brassica oleracea capitata L.
Apium graveolens L. var. dulce Pers.
Primus serotina Ehrh.
Citrus volkameriana Ten. and Pasq.
Trifolium repens L.
Trifolium pratense L.
Zea mays L.
Gossypiwn hirsutum L.
Populus deltoides Marsh
Lepidium sativum L.
Cucumis sativus L.
Rumex obtusifolius L.
Pelargonium x hortorum Bailey
Festuca arundinacea Schreb..
Pseudotsuga menziesii (Mirb.) Franco.
Abies fraseri (Pursh) Poir.
Koelreuteria paniculata Laxm.
Vitis labruscana Bailey
Gleditsia triacanthos L.
Hedera helix L.
Hibiscus cannabinus L.
Juniperus conferta Parl.
Lactuca sativa L.
Syringa vulgaris L.
Beta vulgaris L.
December 1993
 5A-1
DRAFT-DO NOT QUOTE OR CITE

-------
Maple, red
Maple, sugar
Milkweed
Mint
Oak, white
Oak, red
Oats
Onion
Pea
Pepper
Petunia
Pine, Jeffrey
Pine, loblolly
Pine, pitch
Pine, ponderosa
Pine, Scots
Pine, shortleaf
Pine, slash
Pine, white
Plane, London
Poplar
Poplar, hybrid
Poplar, yellow
Potato
Radish
Rape, spring
Sequoia, giant
Sorghum,  hybrid
Soybean
Spinach
Spruce, red
Spruce, Norway
Spruce, sitka
Strawberry, cultivated
Strawberry, wild
Sunflower
Timothy
Tobacco
Tomato
Wheat
Acer rubrum L.
Acer saccharum Marsh
Asclepias spp.
Mentha piperita L.
Quercus alba L.
Quercus rubra L.
Avena sativa L.
Allium cepa L.
Pisum sativum L.
Capsicum annuwn L.
Petunia hybrida Vilm.
Pinus jeffreyi Grev. and Balf.
Pinus taeda L.
Pinus rigida Mill.
Pinus ponderosa Laws.
Pinus sylvestris L.
Pinus echinata Mill.
Pinus elliotti Englem.
Pinus strobus L.
Platanus  x  acerifolia (Ait.) Willd.
Populus nigra L.
Populus maximowicm  x P. trichocarpa
Liriodendron tulipifera L.
Solanwn tuberosum L.
Raphanus sativus L.
Brassica napus L. var. napus
Sequoiadendron giganteum Buchholz
Sorghum bicolor (L.) Moench x
Sorghum x  drummondii (Steudel) Millsp.
and Chase
Gfycine max (L.) Merr.
Spinacea oleracea L.
Picea rubens  Sarg.
Picea abies (L.)  Karst.
Picea sitchensis (Bong.) Carr.
Fragaria x  ananassa Duch.
Fragaria virginiana Duch.
HeUanthus  annuus L.
Phlewn pratense L.
Nicotiana tabacum L.
Lycopercicon escukntum Mill.
Triticum aestivwn L.
December 1993
 5A-2
DRAFT-DO NOT QUOTE OR CITE

-------