EPA/540/2-89/029
SUPERFUND TREATABILITY
CLEARINGHOUSE
Document Reference:
- Canonie Environmental Services Corp. "Soil Remediation and Site Closure McKin
Superfund Site", Gray, Maine. Technical report of approximately 250 pp. prepared for
U.S. EPA. July 1987.
EPA LIBRARY NUMBER:
Superfund Treatability Clearinghouse - EXPE
-------
C-2
Revised Report
MCKIN
702266
PAGE 2
LP-1840
Pyrene
Butylbenzylphthalate
3,3'-Dichlorobenzidine
Benzo(a)Anthracene
bis-(2-Ethylhexyl)Phthalate
Chrysene
Di-N-Octyl Phthalate
Benzo(b)Fluoranthene
Benzo(k)Fluoranthene
Benzo(a)Pyrene
Indenod ,2 ,3-cd)Pyrene
Dibenzo(a,h)Anthracene
BenzoCo.h.i)Pervlene
NO
NO
NO
NO
NO
NO
NO
NO
NO
NO
NO
NO
NO
330
330
660
330
330
330
330
330
330
330
330
330
330
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
Ana 1vat
Checked Bv
CanonleEnvircnmental
-------
Revised Report
Client ID: MCKIN
Sample ID: 64-130-1840
Matrix : SOIL
SAMPLE-3-17-4
Data File:>B2289
3988 702289
GC/MS
SEMI-VOLATILE ANALYSIS
C-3
COMPOUND NAME
AMOUNT
DET. LIMIT
N-Ni t rosodimethylamine
Phenol
bis(-2-Chloroethyl)Ether
2-Chlorooheno1
1 ,3-Dichlorobenzene
1 ,4-Dichlorobenzene
1,2-Dichlorobenzene
bis(2-chloroisoprooyl)Ether
N-Ni troso-Di-Propylami'ne
Hexachloroethane
Nt t robenzene
Isophorone
2-Ni t rooheno1
2.4-Dimethylohenol
bis(-2-Chloroethoxy)Methane
2.4-Dichlorophenol
1.2,4-Trichlorobenzene
Naphthalene
Hexachlorobutadiene
4-Chloro-3-Methylohenol
HexachlorocycloDentadiene
2 ,4,6-Trichloroohenol
2-Chloronaphthalene
Dimethyl Phthalate
Acenaphthylene
2,6-Dinitrotoluene
Acenaphthene
2.4-Dinitroohenol
4-Nit ropheno1
2.4-Dinitrotoluena
Diethylphthalate
4-Chlorophenyl-phenylether
Fluorene
Benz id ine
4,6-Dinitro-2-MethyIpheno1
N-Nit rosodlohenylamine
4-Bromophenyl-phanylether
Hexachlorobenzene
Pentachloroohenol
Phenanthrene
Anthracene
Di-N-Butylphthaiate
Fluoranthene
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
640.
ND
ND
ND
330
330
330
330
330
330
330
330
330
330
330
330
330
330
330
330
330
330
330
330
330
330
330
330
330
330
330
1650
330
330
330
330
330
330
1650
330
330
330
1650
330
330
330
330
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
UQ/KQ
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ua/Ka
CanonleEnvironmental
-------
C-4
Revised Report
rtCKIN
702289 LP-1840
PAGE 2
Pyrene 840. 330 ua/Kg
Butylbenzylohtnalate ND 330 ua/Kg
3.3'-Oichlorobenzidine ND 660 ua/Ka
BenzoCa)Anthracene ND 330 ua/Ka
bis-(2-Ethylhexyl)Phthalate ND 330 ug/Kg
Chrysene 440. 330 ug/Kg
Di-N-Octyl Phthalate ND 330 ug/Kg
Benzo(b)Fluoranthene ND 330 ua/Ka
Benzo(k)Fluoranthene ND 330 ua/Ka
Benzo(a)Pyrene ND 330 ua/Ko
Indenod .2,3-cd)Pyrene ND 330 ug/Ka
Dibenzo(a.h)Anthracene ND 330 uo/Ka
Benzo(g,h,i)Perylene ND 330 ua/Kg
Analvst Checked Bv
CanonleEnvircnmental
-------
Revised Report
Client ID: MCKIN
Sample ID: 84-130-1840
Matrix : SOIL
SAMPLE-3-17-8
Data File
3992 702291
>B2291
GC/MS
SEMI-UOLATILE ANALYSIS
C-5
COMPOUND NAME
AMOUNT
DET. LIMIT
N-Nitrosodimethylaminc
Pheno 1
bis(-2-Chloroethyl)Ether
2-Chloropheno 1
1,3-Dichlorobenzene
1,4-Dichlorobenzene
1,2-Dichlorobenzene
bis(2-chloroisooropy1)Ether
N-Ni t roso-Di-Propylamine
Hexach loroethane
Nit robenzene
Isophorone
2-Ni t ropheno1
2,4-Dimethyl phenol
bis(-2-Chloroethoxy)Methane
2,4-Dichloropheno1
1.2.4-Trichlorobenzene
Naphthalene
Hexachlorobutadiene
4-Chloro-3-Methylohenol
Hexachlorocyclooentadiene
2 ,4.6-Tnchlorophenol
2-Chloronaohthalene
Dimethyl Phthalatc
Acenaohthylene
2 ,6-Dinitrotoluene
Acenaohthene
2,4-Dinitroohenol
4-Ni t ropheno1
2,4-Dinitrotoluena
Diethylphthalate
4-Chloropheny1-phenylether
Fluorene
Benz id ine
4,6-Dinjtro-2-Methylpheno 1
N-Nitrosodiphenylamina
4-Bromopheny1-phenylether
Hexach lorobenzene
Pentachlorophenol
Phenanthrene
Anthracene
Di-N-Butylohthalate
F luoranthene
NO
ND
ND
ND
ND
ND
1300.
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
690.
NO
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
NO
ND
640.
ND
ND
ND
330
330
330
330
330
330
330
330
330
330
330
330
330
330
330
330
330
330
330
330
330
330
330
330
330
330
330
1690
330
330
330
330
330
330
1690
330
330
330
1690
330
330
330
330
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug'Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug'Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
UQ/KQ
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
uo/Ka
CanonleEnvircnmental
-------
Revised Report
MCKIN
702291 LP-1840
PAGE 2
C-6
Pyrene 670.
ButyIbenzylphthalate NO
3 .3'-Dichlorobenzidine NO
Benzo(a)Anthracene ND
bis-(2-Ethylhexyl)Phthalate NO
Chrysene ND
Di-N-Octyl Phthalate NO
Benzo(b )Fluoranthene NO
Benzo(U)Fluoranthene ND
BenzoCa)Pyrene NO
Indenod ,2 .3-cd>Pyrene ND
Dibenzo(a,h)Anthracene ND
BenzoCa ,h,i)Pervlene ND
330
330
660
330
330
330
330
330
330
330
330
330
330
ug/Kg
ug/Kg
ug/Ka
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
Analvst
Checked Bv
CanortleEnviraimental
-------
C-7
Canonie
8703048
Page 2 of
Table 1. Seinivolatile Organic Results
Canonie Sample ID
625 Compounds
Phenol
bis(2-Chloroethyl)Ether
2-Chlorophenol
1,3-Dichlorobenzene
1,4-Dichlorobenzene
1,2-Dichlorobenzene
bis(2-Chloroisopropyl)Ether
N-Nitroso-Oi-n-Propylamine
Hexachloroethane
Nitrobenzene
Isophorone
2-Nitrophenol
2,4-Oimethylphenol
bis(2-Chloroethoxy) Methane
2,4-Dichlorophenol
1,2,4-Trichlorobenzene
Naphthalene
Hexachlorobutadiene
4 -Chi oro-3 -Methyl phenol
Hexachlorocyclopentadiene
2,4,6-Trichlorophenol
2-Chloronaphthalene
Dimethyl Phthalate
Acenaphthylene
Acenaphthene
2,4-Dinitrophenol
4-Nitrophenol
2,4-Dinitrotoluene
2,6-D1n1trotoluene
Diethylphthalate
4-Chlorophenyl-Phenylether
Fluorene
4, 6-Din1tro-2-Methyl phenol
N-Ni trosod iphenyl amlne
4 -Bromopheny 1 -Phenyl ether
Hexachlorobenzene
Pentachlorophenol
Phenanthrene
Anthracene
Di-n-Butylphthalate
3-18-3
ug/kg
<170
<170
<170
<170
<170
<330
<170
<660
<330
<500
<330
<660
<500
<330
<500
<170
<170
<330
<170
<3300
<330
<170
<170
<170
<170
<3300
<1300
<330
<500
<170
<170
<170
<990
<660
<170
<500
<170
590
230
<330
3-19-3
ug/kg
<170
<170
<170
<170
<170
<330
<170
<660
<330
<500
<330
<660
<500
<330
<500
<170
<170
<330
<170
<3300
<330
<170
<170
<170
<170
<3300
<1300
<330
<500
<170
<170
<170
<990
<660
<170
<500
<170
810
180
<330
3-19-15
ug/kg
<170
<170
<170
<170
<170
<330
<170
<660
<330
<500
<330
<660
<500
<330
<500
<170
<170
<330
<170
<3300
<330
<170
<170
<170
<170
<3300
<1300
<330
<500
<170
<170
<170
<990
<660
<170
<500
<170
350
<170
<330
method
blank
ug/kg
<33
<33
<33
<33
<33
<66
<33
<130
<66
<99
<66
<130
<99
<66
<99
<33
<33
<66
<33
<660
<66
<33
<33
<33
<33
<660
<260
<66
<99
<33
<33
<33
<200
<130
<33
<99
<33
<33
<33
<66
-------
C-8
Cancnie
8703048
Page 3 of 3
Table 1. Semivolatile Organic Results (continued)
Canonie Sample ID
625 Compounds
Fluoranthene
Pyrene
Butylbenzylphthalate
3,3-Dichlprobenzidine
Benzo(a)Anthracene
bis(2-Ethylhexyl)Phthalate
Chrysene
Di-n-Octyl Phthalate
Benzo(b) Fl uoranthene
Benzo(k) Fluoranthene
Benzo( a) Pyrene
Indeno(l,2,3-cd)Pyrene
Dibenzo(a.h) Anthracene
Benzo(g,h,i)Pery1ene
Alpha-BHC
Beta-BHC
Gamma-BHC
Delta-BHC
Heptachlor
Aldrin
Heptachlor Epoxide
Endosulfan I
Oieldrin
4,4'-DDE
Endrin
Endosulfan II
4, 4 '-ODD
Endrin Aldehyde
Endosulfan Sulfate
4.4--DDT
PCB's
Surrogates
2-Fluorophenol
Phenol-d5
Nitrobenzene-d5
2-Fluorobiphenyl
2,4,6-Tribromophenol
p-Terphenyl-dl4
3-18-3
ug/kg
<500
<330
<500
<3300
<170
<330
300
<330
<660
<660
<170
<170
<500
<330
<1700
<1700
<1700
<1700
<1700
<1700
<1700
<1700
<1700
<1700
<1700
<1700
<1700
<1700
<1700
<1700
<1700
3-19-3
ug/kg
<500
410
<500
<3300
210
<330
280
<330
<660
<660
<170
<170
<500
<330
<1700
<1700
<1700
<1700
<1700
<1700
<1700
<1700
<1700
<1700
<1700
<1700
<1700
<1700
<1700
<1700
<1700
Percent Recovery
58
58
55
71
63
59
57
59
58
75
66
62
3-19-15
ug/kg
<500
<330
<500
<3300
<170
<330
210
<330
<660
<660
<170
<170
<500
<330
<1700
<1700
<1700
<1700
<1700
<1700
<1700
<1700
<1700
<1700
<1700
<1700
<1700
<1700
<1700
<1700
<1700
(*)
49
57
46
68
64
58
method
blank
ug/kg
<99
<66
<99
<660
<33
<66
<33
<66
<130
<130
<33
<33
<99
<66
<330
<330
<330
<330
<330
<330
<330
<330
<330
<330
<330
<330
<330
<330
<330
<330
<330
72
72
77
85
67
76
-------
Client ID:
Sample 10:
Ma t r i x :
MCKIN
84-139-1856
SOIL
SAMPLE 3-20-12
Data File:>B2481
702481
GC/MS
SEMI-UOLATILE ANALYSIS
C-9
COMPOUND NAME
AMOUNT
DET. LIMIT
N-Nitrosodimethylamme
Pheno1
bis(-2-Chloroethyl)Ether
2-Chloropheno1
1 ,3-Dichlorobenzene
1 ,4-Dichlorobenzene
1 ,2-Dichlorobenzene
bis(2-chloroiaopropyl)Ether
N-Nitroso-Di-Prooylamine
Hexachloroethane
Ni t robenzene
Isoohorone
2-Nit rooheno1
2,4-DimethyIpheno1
bis(-2-Chloroethoxy)Methane
2,4-Dicnloropnenol
1 ,2.4-Trichlorobenzene
Naphtha lene
Hexachlorobutadiene
4-Chloro-3-Methylohenol
Hexachlorocyclooentadiene
2 .4 .6-Tnchlorooheno 1
2-Chloronaohthalene
Dimethyl Phthalate
Acenaohthylene
2,6-Dinitrotoluene
Acenaohthene
2,4-Dinitrooheno1 •
4-Ni t ropheno1
2 ,4-Dinitrotoluene
Diethylphthalate
4-Chlorooheny1-phenylether
Fluorens
Benz id me
4.6-DinitPo-2-MethylohenoI
N-Nitrosodiohenylamine
4-Bromoohenyl-Dhenylether
Hexach lorobenzene
Pentachloroohenol
Phenanthrene
Ant hracene
Di-N-Butyl ohthalate
F luoranthene
NO
ND
NO
NO
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
NO
ND
NO
NO
ND
NO
ND
ND
330
330
330
330
330
330
330
330
330
330
330
330
330
330
330
330
330
330
330
330
330
330
330
330
330
330
330
1650
330
330
330
330
330
330
1650
330
330
330
1650
330
330
330
330
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug'Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug'Kg
ug/Kg
ug/Kg
ug/Kg
ua/Ka
CanonleEnvircnmental
-------
C-10
nCKIN
702481
PAGE 2
LP-1856
Pyrene
Butylbenzylohthalete
3.3'-Dichlorobenzidine
Benzo(a)Anthracene
bis-(2-Ethylhexyl)Phthalate
Chrysene
Di-N-Octyl Phthalate
Benzo(b)Fluoranthene
Benzo(k )Fluoranthene
Benzo(a)Pyrene
Indenod ,2 ,3-cd)Pyrene
Oibenzo(a,h)Anthracene
Benzo(a.h,i)Pervlene
ND
NO
ND
NO
ND
ND
ND
ND
ND
ND
ND
ND
ND
330
330
660
330
330
330
330
330
330
330
330
330
330
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/kg
ug/Kg
ug/Kg
AnaIvst
Checked Bv
CanonieEnvircnmental
-------
C-ll
Canonie
8703053
Page 4 of 5
Table 2. Semivolatile Organic Results
Canonie Sample ID
625 Compounds
3-23-3 3-23-11
ug/kg ug/kg
Phenol <170 <170
bis(2-Chloroethyl)Ether <170 <170
2-Chlorophenol <170 <170
1,3-Oichlorobenzene <170 <170
1,4-Qichlorobenzene <170 <170
1,2-Dichlorobenzene <330 <330
bis(2-Chloroisopropyl)Ether <170 <170
N-Nitroso-Di-n-Propylamine <660 <660
Hexachloroethane <330 <330
Nitrobenzene <500 <500
Isophorone <330 <330
2-Nitrophenol <660 <660
2,4-Oimethylphenol <500 <500
bis(2-Chloroethoxy)Methane <330 <330
2,4-Oichlorophenol <500 <500
1,2,4-Trichlorobenzene <170 <170
Naphthalene <170 <170
Hexachlorobutadiene <330 <330
4-Chloro-3-Methylphenol <170 <170
Hexachlorocyclopentadiene <3300 <3300
2,4,6-Trichlorophenol <330 <330
2-Chloronaphthalene <170 <170
Dimethyl Phthalate <170 <170
Acenaphthylene <170 <170
Acenaphthene <170 <170
2,4-Dinitrophenol <3300 <3300
4-Nitrophenol <1300 <1300
2,4-Dinitrotoluene <330 <330
2,6-Dinitrotoluene <500 <500
Diethylphthalate <170 <170
4-Chlorophenyl-Phenylether <170 <170
Fluorene <170 <170
4,6-Dinitro-2-Methylphenol <990 <990
N-Nitrosod1pheny1am1ne <660 <660
4-8romophenyl-Phenylether <170 <170
Hexachlorobenzene <500 <500
Pentachlorophenol <170 <170
Phenanthrene 560 310
Anthracene 280 <170
Oi-n-Butylphthalate <330 <330
-------
C-12
Canonie
8703053
Page 5 of 5
Table 2. Semivolatile Organic Results (continued)
Canonie Sample ID
625 Compounds
3-23-3 3-23-11
ug/kg ug/kg
Fluoranthene
Pyrene
Butyl benzyl phthal ate
3,3-Dichlorobenzidine
Benzo( a) Anthracene
bis(2-Ethylhexyl) Phthal ate
Chrysene
Oi-n-Octyl Phthalate
Benzo( b) Fl uoranthene
Benzo(k) Fluoranthene
8enzo(a)Pyrene
Indeno(l,2,3-cd)?yrene
Dibenzo( a, h) Anthracene
Benzo(g,h,i)Perylene
Alpha-BHC
Beta-BHC
Gamma -BHC
Delta-BHC
Heptachlor
Aldrin
Heptachlor Epoxide
Endosulfan I
Dieldrin
4,4'-OOE
Endrin
Endosulfan II
4,4'-ODD
Endrin Aldehyde
Endosulfan Sulfate
4,4'-OOT
PCB's
<500
360
<500
<3300
210
<330
310
<330
<660
<660
130
<170
<500
<330
<1700
<1700
<1700
<1700
<1700
<1700
<1700
<1700
<1700
<1700
<1700
<1700
<1700
<1700
<1700
<1700
<1700
<500
<330
<500
<3300
210
<330
210
<330
<660
<660
<170
<170
<500
<330
<1700
<1700
<1700
<1700
<1700
<1700
<1700
<1700
<1700
<1700
<1700
<1700
<1700
<1700
<1700
<1700
<1700
Surrogates
Percent Recovery (X)
2-Fluorophenol
Phenol-d5
Nitrobenzene-d5
2-Fluorobiphenyl
2,4,6-Tribromophenol
p-Terphenyl-d!4
53
58
49
62
20
46
53
50
45
53
10
34
-------
C-13
Client 10:
Sample ID:
Matrix :
MCKIN
84-150-1885
SOIL
SAMPLE 3-24-11
Data File:>B2763
3700 702763
GC/MS
SEMI-VOLATILE ANALYSIS
COMPOUND NAME
N-Ni trosodimethylemine
Phenol
bis(-2-Chloroethyl)Ether
2-Chloropheno1
1.3-Dichlorobenzene
1,4-Dichlorobenzene
1.2-Dichlorobenzene
bis(2-chloroisooropyl)Ether
N-Nitroso-Di-Propylamine
Hexachloroethane
Nitrobenzene
Isophorone
2-Ni t ropheno 1
2 ..4-Dimethylohenol
bis(-2-Chloroethoxy)Methane
2,4-Dichloroohenol
1.2,4-Trichlorobenzene
Naphthalene
Hexachlorobutadiene
4-Chloro-3-Methylphenol
Hexachlorocyclooentadiene
2 .4,6-Tr ichlorophenol
2-Chloronaohthalene
Dimethyl Phthalate
Acenaohthylene
2,6-Dinitrotoluene
Acenaohthene
2.4-0 in itropheno1
4-N» tropheno1
2.4-Dinitrotoluene
Diethylphthalate
4-Chlorophenyl-phenylether
Fluorene
Benzidine
4.6-Dinitro-2-Methylph«nol
N-Nitrosodiphenyl«min«
4-Bromophenyl-phenylether
Hexach lorobenzene
Pentach lorooheno1
Phenanthrene
Anthracene
Di-N-Butylohthalate
Fluoranthene
AMOUNT
DET. LIMIT
ND
ND
ND
ND
ND
ND
ND
ND
NO
ND
ND
ND
ND
ND
ND
NO
ND
NO
ND
NO
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
460.
NO
NO
ND
330
330
330
330
330
330
330
330
330
330
330
330
330
330
330
330
330
330
330
330
330
330
330
330
330
330
330
1650
330
330
330
330
330
330
1650
330
330
330
1650
330
330
330
330
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
UQ/KQ
CanotiieEnviraimental
-------
C-14
MCKIN
702763
PAGE 2
LP-1&85
Pyrane 510.
ButyIbenzylohthalata NO
3.3'-Dichlorobenzidina NO
Benzo(a)Anthracane NO
bis-(2-Ethylhexyl)Phthalate NO
Chrysene NO
Di-N-Octyl Phthalate NO
Benzo(b)Fluoranthena NO
Benzo(k)Fluoranthene NO
Benzo(a)Pyrane NO
Indeno(1.2,3-cd)Pyrane NO
Dibenzo(a,h)Anthracene NO
BenzoCq,h,»>Pervl«ne NO
330
330
660
330
330
330
330
330
330
330
330
330
330
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
UQ/KQ
.Jk...
Ana 1vst
Checked Bv
CanonleEnvircnmental
-------
Client ID:
Sample 10:
Matrix :
MCKIN
84-130-1889
SOIL
SAMPLE 3-25-3
Data File:>B2764
3206 702764
GC/MS
SEMI-VOLATILE ANALYSIS
C-15
COMPOUND NAME
AMOUNT
DET. LIMIT
N-Nitrosodime thylamina
Phenol
bis(-2-Chloroethyl)Ether
2-Chloroohenol
1,3-Dichlorobenzene
1,4-Dichlorobenzene
1.2-Diehlorobenzene
bis(2-chloroisoDropyl)Ether
N-Nitroso-Di-Propylamine
Hexachloroethane
Nit robenzene
Isoohorone
2-Ni t rooheno1
2.4-Dime thy1 phono1
bis(-2-Chloroethoxy)Methane
2,4-Dichloroohenol
1.2,4-Trichlorobenzene
Naohthalene
Hexachlorobutadiene
4-Chloro-3-MethyIpheno1
Hexachlorocyclooentadiene
2,4.6-Trichlorooheno1
2-Chloronaohthalene
Dimethyl Phthalate
Acenaohthylene
2 ,6-Dinitrotoluene
Acenaohthene
2 . 4-Din11rophenol
4-Ni t rooheno1
2.4-Dinitrotoluene
Diethylohthalata
4-Chloropheny1-phanylether
Fluorena
Benzidina
4.6-Din it ro-2-MathyIpheno1
N-Nitrosodiohenylamina
4-Bromophenyl-phenylether
Hexachlorobenzena
Pentachlorooheno1
Phenanthrene
Anthracene
Di-N-Butylphthalate
Fluoranthene
ND
ND
ND
ND
ND
ND
ND
NO
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
570.
ND
ND
380.
330
330
330
330
330
330
330
330
330
330
330
330
330
330
330
330
330
330
330
330
330
330
330
330
330
330
330
1650
330
330
330
330
330
330
1650
330
330
330
1650
330
330
330
330
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
UQ/KQ
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
UQ/KQ
CanonleErwironmental
-------
C-16
MCKIN
702764
PAGE 2
LP-1885
Pyrene
Butylbenzylphthalate
3,3'-Dichlorobenzidine
Benzo(a)Anthracene
bis-(2-Ethylhexyl)Phthalati
Chrysene
Di-N-Octyl Phthalate
Benzo(b)Fluoranthene
Benzo(k)Fluoranthene
Benzo(a)Pyrene
Indeno(1,2 ,3-cd)Pyrene
Dibenzo(a ,h)Anthracene
Benzo(g ,h , i)Perylene
650.
ND
NO
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
330
330
660
330
330
330
330
330
330
330
330
330
330
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
uaXKa
ug/Kg
ug/Kg
ug/Kg
Ana 1v»t
Checked Bv
CanorteEnvircnmental
-------
Client ID:
Samole ID:
Ma t r i x :
MCKIN
84-130-188?
SOIL
SAMPLE 3-25-14
Data
3219
File:>B2765
702765
GC/MS
SEMI-UOLATILE ANALYSIS
C-17
COMPOUND NAME
AMOUNT
DET. LIMIT
N-Nitrosodimethylamine
Phenol
bia(-2-Chloroethyl)Ether
2-Chloroohenol
1.3-Dichlorobenzene
1,4-Dichlorobenzene
1,2-Dichlorobenzene
bis(2-chloroisopropyl)Ether
N-Nitroso-Di-Propylanune
Hexachloroethane
Nit robenzene
Isoohorone
2-Ni t ropheno 1
2,4-Dimethylphenol
bi»(-2-Chloroethoxy)Methane
2,4-Dichlorophenol
1.2,4-Trichlorobenzene
Naphthalene
Hexachlorobutadiene
4-Chloro-3-Methylphenol
Hexachlorocyclopentadiene
2.4,6-Trichloroohenol
2-Chloronaphthalene
Dimethyl Phthalate
Acenaohthylene
2 .6-Dinitrotoluene
Acenaphthene
2.4-0 in itropheno 1
4-Ni tropheno1
2.4-Dinitrotoluene
Diethylphthalate
4-Chlorooheny1-phenylether
Fluorene
Benz id ine
4,6-Dinit ro-2-Methylpheno1
N-Nitrosod iphenylamine
4-Bromopheny1-phenylether
Hexach lorobenzene
Pentach loropheno1
Phenanthrene
Anthracene
Di-N-Butylphthalate
Fluoranthene
ND
NO
ND
ND
ND
ND
ND
NO
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
600.
ND
NO
380.
330
330
330
330
330
330
330
330
330
330
330
330
330
330
330
330
330
330
330
330
330
330
330
330
330
330
330
1650
330
330
330
330
330
330
1650
330
330
330
1650
330
330
330
330
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
uqXKg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
UO/KQ
CanonteEnvironmental
-------
C-18
MCKIN
702765
PAGE 2
LP-1S85
Pyrene 580.
ButyIbenzylohtha late NO
3,3'-Dichlorobenzid me NO
Benzo(a)Anthracene ND
b»s-(2-Ethylhexyl>Phthelate ND
Chrysene NO
Di-N-Octyl Phthalate ND
Benzo (b )'F luoranthene ND
Benzo(k )Fluoranthene ND
Benzo(a)Pyrene ND
Indenod .2 ,3-cd)Pyrene ND
DibenzoCa,h>Anthracene ND
Benzo(Q,h.i)Pervlene ND
330
330
660
330
330
330
330
330
330
330
330
330
330
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
Ana 1vst
Checked Bv
CanonteEnvircnmental
-------
Canonie
8703065
Page 4 of 7
C-19
Table 2. Semivolatile Organic Results
Canom'e Sample 10
625 Compounds
3-17-6 3-17-10 3-17-14 3-26-2 3-26-5
• •»•••••«• • ••••••• • ••••»•«•• • •••••••• • •••*•«•
ug/kg ug/kg ug/kg ug/kg ug/kg
Phenol
bis(2-Chloroethyl)Ether
2-Chloro phenol
1,3-Dichlorobenzene
1,4-Oichlorobenzene
1,2-Oichlorobenzene
bis(2-Chloroisopropyl)Ether
N-Nitroso-Di-n-Propylamine
Hexachloroethane
Nitrobenzene
Isophorone
2-Nitrophenol
2,4-Oimethylphenol
bis(2-Chloroethoxy) Methane
2,4-Dichlorophenol
1,2,4-Trichlorobenzene
Naphthalene
Hexachlorobutadiene
4-Chloro-3-Methyl phenol
Hexachlorocyclopentadiene
2,4,6-Tn'chlorophenol
2-Chloronaphthalene
Dimethyl Phthalate
Acenaphthylene
Acenaphthene
2,4-Dinitrophenol
4-Nitrophenol
2,4-Oinitrotoluene
2,6-Oinitrotoluene
Diethylphthalate
4-Chl orophenyl -Phenyl ether
Fluorene
4,6-Din1tro-2-Methylphenol
N-Nitrosod1phenylam1ne
4-8romophenyl -Phenyl ether
Hexachlorobenzene
Pentachlorophenol
Phenanthrene
Anthracene
Di-n-Butylphthalate
<170
<170
<170
<170
<170
<330
<170
<660
<330
<500
<330
<660
<500
<330
<500
<170
<170
<330
<170
<3300
<330
<170
<170
<170
<170
<3300
<1300
<330
<500
<170
<170
<170
<990
<660
<170
<500
<170
280
<170
<330
<170
<170
<170
<170
<170
<330
<170
<660
<330
<500
<330
<660
<500
<330
<500
<170
<170
<330
<170
<3300
<330
<170
<170
<170
<170
<3300
<1300
<330
<500
<170
<170
<170
<990
<660
<170
<500
<170
<170
<170
<330
<170
<170
<170
<170
<170
<330
<170
<660
<330
<500
<330
<660
<500
<330
<500
<170
<170
<330
<170
<3300
<330
<170
<170
<170
<170
<3300
<1300
<330
<500
<170
<170
<170
<990
<660
<170
<500
<170
360
<170
<330
<170
<170
<170
<170
<170
<330
<170
<660
<330
<500
<330
<660
<500
<330
<500
<170
<170
<330
<170
<3300
<330
<170
<170
<170
<170
<3300
<1300
<330
<500
<170
<170
<170
<990
<660
<170
<500
<170
280
300
<330
<170
<170
<170
<170
<170
<330
<170
<660
<330
<500
<330
<660
<500
<330
<500
<170
<170
<330
<170
<3300
<330
<170
<170
<170
<170
<3300
<1300
<330
<500
<170
<170
<170
<990
<660
<170
<500
<170
230
250
<330
-------
C-20
Canonie
8703065
Page 5 of 7
Table 2. Semivolatile Organic Results (continued)
Canonie Sample 10
3-17-6 3-17-10 3-17-14 3-26-2 3-26-5
625 Compounds
Fluoranthene
Pyrene
Butyl ben zylphthal ate
3,3-Dichlorobenzidine
Benzo(a)Anthracene
bis(2-Ethylhexyl)Phthalate
Chrysene
Oi-n-Octyl Phthalate
Benzo(b) Fluoranthene
Benzo( k) Fl uoranthene
Benzo(a)Pyrene
Indeno(l, 2, 3-cd) Pyrene
Dibenzo( a, h) Anthracene
Benzo(g,h,i)Perylene
Alpha-BHC
Beta-BHC
Gamma-BHC
Delta-BHC
Heptachlor
Aldrin
Heptachlor Epoxide
Endosulfan I
Dieldrin
4, 4 '-DDE
Endrin
Endosulfan II
4,4'-DDD
Endrin Aldehyde
Endosulfan Sulfate
4, 4 '-DOT
PCB's
Surrogates
2-Fluorophenol
Phenol-d5
Nitrobenzene-d5
2-Fluorobiphenyl
2,4,6-Tribromophenol
p-Terphenyl-d!4
ug/kg
<500
<330
<500
<3300
<170
860
<170
<330
<660
<660
<170
<170
<500
<330
<1700
<1700
<1700
<1700
<1700
<1700
<1700
<1700
<1700
<1700
<1700
<1700
<1700
<1700
<1700
<1700
<1700
Percent
60
60
60
60
50
60
ug/kg
<500
<330
<500
<3300
<170
580
<170
<330
<660
<660
<170
<170
<500
<330
<1700
<1700
<1700
<1700
<1700
<1700
<1700
<1700
<1700
<1700
<1700
<1700
<1700
<1700
<1700
<1700
<1700
Recovery (I)
25
20
20
30
5
30
ug/kg
<500
<330
<500
<3300
<170
640
<170
<330
<660
<660
<170
<170
<500
<330
<1700
<1700
<1700
<1700
<1700
<1700
<1700
<1700
<1700
<1700
<1700
<1700
<1700
<1700
<1700
<1700
<1700
55
50
50
50
40
90
ug/kg
<500
<330
<500
<3300
<170
960
<170
<330
<660
<660
<170
<170
<500
<330
<1700
<1700
<1700
<1700
<1700
<1700
<1700
<1700
<1700
<1700
<1700
<1700
<1700
<1700
<1700
<1700
<1700
60
55
50
60
30
50
ug/kg
<500
<330
<500
<3300
<170
360
<170
<330
<660
<660
<170
<170
<500
<330
<1700
<1700
<1700
<1700
<1700
<1700
<1700
<1700
<1700
<1700
<1700
<1700
<1700
<1700
<1700
<1700
<1700
45
40
40
50
35
40
*Surrogate recovery values are somewhat imprecise due to a five fold dilution
of each extract. In addition, some of sample 3-17-10 was lost in the
preparation step resulting in a lower recovery of all analytes as indicated
by the lower surrogate recoveries.
-------
C-21
Canonie
8703065
Page 6 of
Table 2. Semivolatile Organic Results
Canonie Sample ID
method
blank
625 Compounds ug/kg
Phenol <33
bis(2-Chloroethy1)Ether <33
2-Chlorophenol <33
1,3-Dichlorobenzene <33
1,4-Dichlorobenzene <33
1,2-Dichlorobenzene <66
bis(2-Chloroisopropyl)Ether <33
N-Nitroso-Oi-n-Propylamine <130
Hexachloroethane <66
Nitrobenzene <99
Isophorone <66
2-Nitrophenol <130
2,4-Dimethylphenol <99
bis(2-Chloroethoxy)Methane <66
2,4-Oichlorophenol <99
1,2,4-Trichlorobenzene <33
Naphthalene <33
Hexachlorobutadiene <66
4-Chloro-3-Methylphenol <33
Hexachlorocyclopentadiene <660
2,4,6-Trichlorophenol <66
2-Chloronaphthalene <33
Dimethyl Phthalate <33
Acenaphthylene <33
Acenaphthene <33
2,4-Dinitrophenol <660
4-Nitrophenol <260
2,4-Dinitrotoluene <66
2,6-D1nitrotoluene <99
Diethylphthalate <33
4-Chlorophenyl-Phenylether <33
Fluorene <33
4,6-D1n1tro-2-Methylphenol <200
N-Nitrosod1phenylam1ne <130
4-Bromophenyl-Phenylether <33
Hexachlorobenzene <99
Pentachlorophenol <33
Phenanthrene <33
Anthracene <33
Di-n-Butylphthalate <66
-------
C-22
Canonie
8703065
Page 7 of 7
Table 2. Semivolatile Organic Results (continued)
Canonie Sample 10
method
blank
625 Compounds ug/kg
Fluoranthene <99
Pyrene <66
Butyl benzylphthalate <99
3,3-Dichlorobenzidine <660
8enzo(a)Anthracene <33
bis(2-Ethylhexyl)Phthalate 160
Chrysene <33
Oi-n-Octyl Phthalate <66
Benzo(b)Fluoranthene <130
8enzo(k)Fluoranthene <130
Benzo(a)Pyrene <33
Indeno(l,2,3-cd)Pyrene <33
Dibenzo(a,h)Anthracene <99
Benzo(g,h,i)Perylene <66
Alpha-BHC <330
Beta-BHC <330
Gamma-BHC <330
Oelta-BHC <330
Heptachlor <330
Aldrin <330
Heptachlor Epoxide <330
Endosulfan I <330
Oieldrin <330
4,4'-DDE <330
Endrin <330
Endosulfan II <330
4,4'-ODD <330
Endrin Aldehyde <330
Endosulfan Sulfate <330
4,4'-DDT <330
PCB's <330
Surrogates Percent Recovery (X)
2-Fluorophenol 61
Phenol-d5 53
Nitrobenzene-d5 62
2-Fluorobiphenyl 64
2,4,6-Tribromophenol 45
p-Terphenyl-d!4 82
-------
Client ID:
Sample ID:
Matrix :
MCKIN
84-130-1912
SOIL
SAMPLE 3
-27-2$
Data
3279
File:>83070
703070
GC/MS
SEMI -VOLATILE ANALYSIS
C-23
COMPOUND NAME
AMOUNT
DET. LIMIT
N-Nitrosodimethylamine
Phenol
bis(-2-Chloroethyl)Ether
2-Chlorooheno 1
1,3-Dichlorobenzene
1,4-Dichlorobenzene
1,2-Dichlorobenzene
bis(2-chloroisooropyl)Ether
N-Ni t roso-Di-Propylamine
Hexach loroethane
Nitrobenzene
Isophorone
2-Nitrophenol
2. 4-DimethyIpheno1
bis(-2-Chloroethoxy)Methane
2,4-Dichlorooheno1
1.2.4-Trichlorobenzene
Naphthalene
Hexachlorobutadiene
4-Chloro-3-Methylphenol
Hexachlorocyclopentadiene
2.4.6-Trichlorooheno1
2-Chloronaphthalene
Dimethyl Phthalate
Acenaphthylene
2.6-Dinitrotoluene
Acenaphthene
2,4-Din i t ropheno1
4-Nit ropheno1
2,4-Dinitrotoluene
Oiethylphthalate
4-Chlorophenyl-phenylether
Fluorene
Benzidine
4,6-Dinitro-2-MethyIpheno 1
N-Njtrosodiphenylamine
4-Bromopheny1-phenylether
Hexachlorobenzene
Pentachlorophenol
Phenanthrene
Anthracene
Di-N-Butylohthe late
Fluoranthene
ND
NO
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
NO
ND
NO
NO
780.
1600.
ND
550.
330
330
330
330
330
330
330
330
330
330
330
330
330
330
330
330
330
330
330
330
330
330
330
330
330
330
330
1650
330
330
330
330
330
330
1650
330
330
330
1650
330
330
330
330
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
UQ/KQ
CanonloEnvircnmental
-------
C-24
MCKIN
703070
PAGE 2
LP-1912
Pyrene 690.
ButyIbenzylphthalate ND
3,3'-Dichlorobenzidine NO
Benzo(a)Anthracene 910.
bis-<2-Ethylhexyl)Phthelate ND
Chrysene 860.
Di-N-Octyl Phthalate NO
BenzoCb)Fluoranthane ND
Benzo(k)Fluoranthene ND
BenzoCaJPyrene ND
Indenod ,2,3-cd)Pyrene ND
Dibenzo(a.h)Anthracene ND
BenzoCg .h,iJPerylene ND
330
330
660
330
330
330
330
330
330
330
330
330
330
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Ka
ug/Kg
ug/Kg
ug/Kg
ug/Ka
ug/Kg
ug/Kg
ug/Kg
ua/Ka
Analyst
Checked Bv
CanoiUeEnvircnmental
-------
Client ID:
Sample ID:
ha t r i x :
MCKIN
84-130-1926
SOIL
SAMPLE 3-27-6
Data File:>B3156
3244 703156
GC/MS
SEMI-VOLATILE ANALYSIS
C-25
COMPOUND NAME
AMOUNT
DET. LIMIT
N-Nitrosodimethylamine
Phenol
bis(-2-Chloroethyl>Ether
2-Chloropheno1
1,3-Dichlorobenzene
1.4-Dichlorobenzene
1,2-Dichlorobenzene
bis(2-chloro isopropy1)Ether
N-Nitroso-Di-Propylemine
Hexach loroethane
Ni t robenzene
Isophorone
2-Ni tropheno1
2,4-Dimethylphenol
bi»(-2-Chlopoethoxy)Methane
2,4-Dichloropheno1
1.2.4-Trichlorobenzene
Naphtha lene
Hexach lorobutadiene
4-Chloro-3-Methylphenol
Hexachlorocyclopentadiene
2,4.6-Trichloropheno1
2-Chloronaphthalene
Dimethyl Phthalate
Acenaphthylene
2.6-Dinitrotoluene
Acenaphthene
2.4-0 in itropheno1
4-Nitrophenol
2 ,4-Oinitrotoluene
Diethylphthalate
4-Chlorophenyl-phenylether
Fluorene
Benz id ine
4.6-Dinitro-2-Methy1phenol
N-Nitrosodiphenylamina
4-Bromopheny1-phenylether
Hexach lorobenzene
Pentach loropheno1
Phenanthrene
Anthracene
Di-N-Butylphthai ate
Fluoranthene
ND
NO
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
NO
ND
ND
350.
ND
ND
330
330
330
330
330
330
330
330
330
330
330
330
330
330
330
330
330
330
330
330
330
330
330
330
330
330
330
1650
330
330
330
330
330
330
1650
330
330
330
1650
330
330
330
330
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
UO/KQ
CanonieEnviraimental
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C-26
HCKIN
703156
PAGE 2
LP-1926
Pyrene 570.
Butylbenzylphthalate NO
3 ,3'-Dichlorobenzidine NO
Benzo(e^Anthracene ND
bia-(2-Ethylhexyl)Phthalate ND
Chrysene NO
Di-N-Octyl Phthalate ND
Benzo(b)Fluoranthene NO
Benzo(k>Fluoranthene NO
Benzo(a)Pyrene NO
Indenod ,2,3-cd>Pyrene ND
Dibenzo(a ,n)Anthracene NO
Benzo(g,h.i)Perylene NO
330
330
660
330
330
330
330
330
330
330
330
330
330
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Ka
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ua/Ka
A6AI.
Ana 1vst
Checked Bv
CanomeEnvircnmentdl
-------
Client ID:
Sample 10:
Ma t r i x :
MCKIN
84-130-1926
SOIL
SAMPLE 3-30-4
Data File:>B3159
3297 703159
GC/MS
SEMI-VOLATILE ANALYSIS
C-27
COMPOUND NAME
AMOUNT
DET. LIMIT
N-Ni t rosod imethylamme
Phenol
bis(-2-Chloroethyl)Ether
2-Chlorophenol
1,3-Dichlorobenzena
1.4-Dichlorobenzene
1,2-Dichlorobenzene
bis(2-chloroisooropyl)Ether
N-Nitroso-Di-Propylamine
Hexachloroethane
Ni t robenzene
Isophorone
2-Ni t ropheno1
2,4-Dimethylphenol
bis(-2-Chloroethoxy)Methane
2.4-Dichlorophenol
1,2,4-Tr ichlorobenzene
Naphthalene
Hexachlorobutadiene
4-Chloro-3-Methylpheno1
Hexachlorocyclopentadiene
2.4.6-Trichloropheno1
2-Chloronaphthalene
Dimethyl Phthalate
Acenaphthylene
2.6-Dinitrotoluene
Acenaohthene
2,4-D i n11 ropheno1
4-Ni t ropheno 1
2.4-0in itrotoluene
Diethylphthalate
4-Chlorophenyl-phenylether
Fluorene
Benz idine
4,6-Dinitro-2-hethylph»nol
N-Nitrosodiphenylamine
4-Bromophenyl-phenylether
Hexach lorobanzene
Pentachloropheno1
Phenanthrene
Anthracene
Di-N-Butylphthe late
Fluoranthene
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
440.
480.
NO
ND
330
330
330
330
330
330
330
330
330
330
330
330
330
330
330
330
330
330
330
330
330
330
330
330
330
330
330
1650
330
330
330
330
330
330
1650
330
330
330
1650
330
330
330
330
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
UQ/KQ
ug/Kg
ug/Ka
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Ka
ug/Kg
ug/Kg
ug/Kg
ug/Ka
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
CanonleEnvironmental
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SUPERFUND TREATABILIT7 CLEARINGHOUSE ABSTRACT
Treatment Process;
Media:
Document Reference:
Document Type:
Contact:
Site Name:
Location of Test:
Physical/Chemical - Low Temperature Thermal
Stripping
Soil/Generic
Canonie Environmental Services Corp. "Soil
Remediation and Site Closure McKin Superfund Site",
Gray, Maine. Technical report of approximately 250
pp. prepared for U.S. EPA. July 1987.
Contractor/Vendor Treatability Study
U.S. EPA - Region I
John F. Kennedy Federal Bldg.
Room 2203
Boston, MA 02203
617-565-3715
McKin Superfund Site, Gray, ME (NPL)
Gray, ME
BACKGROUND; This treatability study report describes soil remediation and
site closure activities conducted at the McKin Superfund site in Maine.
The work described in this report involves the removal of volatile organic
compounds and petroleum residues from contaminated soils by low temperature
thermal aeration in an enclosed environment. The report discusses the
enclosed aeration process, impact of the operation on ambient air quality,
effectiveness of the system, cleanup costs, and disposal of accumulated
on-site materials used in the project.
OPERATIONAL INFORMATION; The soil aeration system utilized during the site
cleanup consisted of a thermal dryer, a baghouse for control of particulate
matter, a scrubber to remove water soluble gases, and a vapor phase carbon
treatment system to remove organics from the vapor phase. Soils were
screened to remove boulders and debris, and fed through the system a number
of times via a conveyer to ensure complete aeration. Soil temperatures
were maintained at 250 - 400°F to facilitate volatilization of organics.
Soil was solidified with concrete after treatment. 11,500 cubic yards of
soil were processed at the site. Soil types are discussed in reports on
previous studies conducted on the site. Organic vapor concentrations were
monitored at the site boundaries, periodic air quality monitoring was
conducted at 10 nearby residences and high volume particulate sampling was
conducted at the site. Ambient hydrocarbon levels were well below (between
0.002 to 0.01 ppm) the level established as a health standard (2 ppm).
During the pilot study, ambient particulate standards were exceeded on
three occasions. Changes in the material handling system reduced fugitive
dust emissions and allowed for the processing of 10,000 cubic yards of
soils without further exceedences of the air quality standard for total
solid particles. Various references are made to QA/QC and to the EPA
standard methods for VOC analysis.
3/89-31 Document Number: EXPE
NOTE: Quality assurance of data may not be appropriate for all uses.
-------
PERFORMANCE; The excavated/aerated soils from the site satisfy the
performance standard specified in the site Record of Decision (ROD)(0.1 ppm
of TCE). Concentrations of VOCs and petroleum products before and after
treatment of soils are shown in Table 1.
Significant reduction in the levels of various contaminants before and
after treatment are noted. Groundwater modeling demonstrated that
groundwater criteria specified in the ROD were met. A detailed cost
breakdown of the use of aeration to remediate soils contaminated with VOC
and petroleum hydrocarbons is provided. Based on this data, the average
cost for treating the soils at this Superfund site is $252 per cubic yard.
Aeration was utilized to remediate contaminated soil and not violate
ambient air quality criteria at this site.
CONTAMINANTS;
Analytical data is provided in the treatability study report.
breakdown of the contaminants by treatability group is:
The
Treatability Group
WOl-Halogenated Aromatic
Compounds
W04-Halogenated Aliphatic
Solvents
W07-Heterocyclics and
Simple Aromatics
W08-Polynuclear Aromatics
W09-0ther Polar Organic
Compounds
W13-0ther Organics
CAS NUMBER
95-50-1
71-55-6
75-35-4
127-18-4
79-01-6
71-43-2
100-41-4
108-88-3
1330-20-7
120-12-7
91-20-3
206-44-0
85-01-8
85-68-7
78-59-1
TEH
Contaminants
1,2-Dichlorobenzene
1,1,1-Trichloroethane
1,1-Dichloroethene
Te t rachloroe thene
Trichloroethene
Benzene
Ethylbenzene
Toluene
Xylene
Anthracene
Naphthalene
Fluoranthene
Phenanthrene
Butylbenzylphthalate
Isophorone
Total Extractable Hydro-
carbons
3/89-31 Document Number: EXPE
NOTE: Quality assurance of data may not be appropriate for all uses.
-------
TABLE 1
Compound Pretreatment Soil
Concentration
(rag/kg)
trans 1. 1, -dichloroethane
trichloroethene (TCE)
1,1,1 , -trichloroethene
Toluene
Xylenes
0.11
7.3
0.13
35
84
Post-treatment Soil
Concentration
(mg/kg)
ND
ND
ND
ND
ND
.02
.02
.02
1.0
1.0
ND - None detected at 0.2 or 1.0 ppm
Note: This is a partial listing of data. Refer to the document for more
information.
3/89-31 Document Number: EXPE
NOTE: Quality assurance of data may not be appropriate for all uses.
-------
Report
Soil Remediation and
Site Closure
McKin Superfund Site
CanonieEnvircnmental
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TABLE OF CONTENTS
PAGE
LIST OF TABLES i
LIST OF FIGURES ii
LIST OF APPENDICES iii
1.0 INTRODUCTION AND CHRONOLOGY 1
2.0 ENCLOSED ENVIRONMENT AERATION SYSTEM 3
3.0 AIR MONITORING 5
3.1 Contingency Actions 8
4.0 EXCAVATION TECHNIQUES UTILIZED 9
4.1 Excavation of Soils Containing VOCs 9
4.2 Excavation of Soils Containing Petroleum 12
5.0 PROCESSING PARAMETERS 14
5.1 Processing Parameters for Soils Containing VOCs 14
5.2 Processing Parameters for Soils Containing Petroleum 15
6.0 ANALYTICAL VERIFICATION 16
6.1 Analytical Verification of Treated Soils from VOC Areas 16
6.2 Analytical Verification of Treated Soils from Petroleum
Areas 17
6.3 Analytical Verification of Excavated Areas 18
6.4 QA/QC Documentation 19
7.0 REMEDIATION OF SOILS 20
7.1 Remediation of Soils Containing VOCs 20
7.2 Remediation of Petroleum Areas 21
7.3 Hydrocarbon Fate and Ground Water Transport 22
8.0 SUBSEQUENT ON-SITE ACTIONS FOR PROTECTION 25
OF PUBLIC HEALTH, WELFARE, AND ENVIRONMENT
9.0 SITE DEMOBILIZATION AND CLOSURE 26
CanomeEnvironmerlai
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TABLE OF CONTENTS
(Continued)
PAGE
10.0 OFF-SITE DISPOSAL OF ACCUMULATED MATERIALS 28
11.0 COST BREAKDOWN FOR AERATION OF SOILS 30
12.0 SUMMARY 31
REFERENCES
TABLES
FIGURES
APPENDIX A
APPENDIX B
APPENDIX C
APPENDIX D
APPENDIX E
APPENDIX F
APPENDIX G
APPENDIX H
CanonieEnvironn'
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LIST OF TABLES
TABLE
NUMBER TITLE
1 Summary of Excavation and Treatment Data -
Areas 3 and 6
2 Summary of Excavation and Treatment Data -
Areas l(b), 4, and 8
3 Summary of TCE Concentrations - Excavation
Perimeter Samples
4 VOC Areas Excavation Verification Analysis
5 Excavation Perimeter Sample Elevations,
Areas 1 (a, c), 2, and 9
6 Petroleum Areas Excavation Verification Analysis
7 Summary of Petroleum Area Soils Aeration
8 Summary of Petroleum Area Soils Aeration, Post-
Treatment Analytical Results
9 Cost Breakdown for Aeration of Areas l(b), 3, 4,
6, and 8
10 Cost Breakdown for Aeration of Areas l(a, c), 2,
and 9
11 Summary of Soil Volumes Excavated and Treated
CanonieEnvironmt
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n
LIST OF FIGURES
FIGURE DRAWING
NUMBER NUMBER TITLE
1 CH84-130-E88 Areas of Excavation
2 CH84-130-E83 Area l(b) Excavation and Perimeter Sample
Locations
3 CH84-130-E87 Area 3 Excavation
4 CH84-130-E80 Area 3 Perimeter Sample Locations
5 CH84-130-E84 Area 4 Excavation and Perimeter Sample
locations
6 CH84-130-E81 Area 6 Excavation
7 CH84-130-E82 Area 6 Perimeter Sample Locations
8 CH84-I30-E85 Area 8 Excavation and Perimeter Sample
Locations
9 CH84-I30-E92 Areas 1 (a, c) Excavation and Perimeter Sample
Locations
10 CH84-130-E90 Area 2 Excavation and Perimeter Sample
Locations
11 CH84-130-E91 Area 9 Excavation and Perimeter Sample
Locations
12 CH84-130-E93 Deposition Area for Treated Petroleum Soils
13 CH84-130-E86 Lagoon Excavation and Deposition Area
14 CH84-130-E89 Final Elevation Contours
CanonleErrv ircnmenta:
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m
LIST OF APPENDICES
APPENDIX A
APPENDIX B
APPENDIX C
APPENDIX D
APPENDIX E
APPENDIX F
APPENDIX G
APPENDIX H
Miscellaneous Laboratory Analytical Reports
Excavation, Sampling and Analytical Verification
- Petroleum Areas 1 (a, c) and 2
Laboratory Analytical Reports - Petroleum Area
Soil Aeration, U.S. EPA Method 8270 and Total
Extractable Hydrocarbons
Quality Assurance Data - McKin/Stockton,
California Laboratory Analytical Comparison
Comparison of Pre-Treatment and Post-Treatment
Soil Characterization - Soils Containing VOCs
Comparison of Pre-Treatment and Post-Treatment
Soil Characterization - Petroleum Area Soils
Decontamination Certification
Manifest Forms - Transportation and Disposal of
Waste Materials
CanonieEnvironrr
-v-4--
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REPORT
SOIL REMEDIATION AND SITE CLOSURE
MCKIN SUPERFUND SITE
GRAY, MAINE
1.0 INTRODUCTION AND CHRONOLOGY
This report by Canonic Environmental Services Corp. (Canonie) describes
soil remediation and site closure activities conducted at the McKin
Superfund Site in Gray, Maine. This report is submitted in response to the
May 12, 1987 letter request of the United States Environmental Protection
Agency (U.S. EPA) and in satisfaction of Paragraph 31(g) of the July 7,
1986, Administrative Order issued by U.S. EPA to the Potentially
Responsible Parties (PRPs) for the McKin site.
The soil remediation described in this report involved the removal of
volatile organic compounds (VOCs) and petroleum residues from soil through
low temperature thermal aeration in an enclosed environment. Pursuant to a
previous Administrative Order dated August 23, 1985, Canonie conducted a
pilot study of the aeration technique, and demonstrated its effectiveness
for the treatment of soils at the site without adverse impacts on the
ambient air quality at the site. The methods and results of the full-scale
aeration program are presented in this report.
Following the submittal of the soil aeration pilot study report in April,
1986, Canonie began full-scale aeration of soils on July 8, 1986, in
accordance with U.S. EPA's 22 conditions for continuing aeration. The
conditions were attached to the July 7, 1986, Administrative Order.
Canonie submitted the excavation plan for VOC-impacted soils on July 11,
1986, with clarifications thereto following. Aeration of VOC-impacted
soils was completed on February 3, 1987. The "Petroleum Area Soils
Characterization and Remediation Analysis" was submitted in January, 1987,
with subsequent approval to proceed with aeration of petroleum area soils
received from U.S. EPA and MDEP on March 13, 1987. Aeration of petroleum
area soils was completed on April 17, 1987. Site demobilization and final
closure followed and was completed on June 23, 1987.
CanonieEnvironmentc
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The balance of this report details the procedures used to successfully
excavate and treat soils known to have been impacted by VOCs and petroleum
residues, and summarizes the data which indicates that proper remediation
has been attained.
CanonieEnvironme
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2.0 ENCLOSED ENVIRONMENT AERATION SYSTEM
The aeration system assembled and utilized during the soil aeration pilot
study is described in detail in the report entitled, "Soil Aeration Pilot
Study", dated April, 1986. The components of the system are a thermal
dryer, a baghouse for particulate control, a scrubber to remove water-
soluble gases, and a vapor phase carbon treatment system to remove organics
from the exhaust air stream. Soil is fed through the system numerous times
for complete aeration.
During the pilot study, three conveyors were employed to feed newly
excavated soil into the aeration system and to reelrculate treated soils
for further aeration. The use of the three conveyors resulted in the
generation of fugitive dust each time the treated soil was discharged from
one conveyor onto another conveyor. Additionally, the cycle time for
treatment of the soil was dependent upon the time required to transport the
soil and to minimize dust generation. Prior to commencement of full-scale
operations in the treatment of soils at the McKin site, Canonie completed
certain modifications to the material handling system, to increase the
efficiency of the system, and reduce the generation of fugitive dust.
Fugitive dust generation was significantly reduced by using a bucket
elevator and chute arrangement. The bucket elevator was positioned
adjacent to the discharge of the materials dryer and transported the
treated soil from the discharge of the dryer up to an enclosed chute which
sloped down to the inlet end of the dryer or to a system discharge
location. A slurry box was mounted near the inlet end of the materials
dryer. A small auger was mounted between the discharge of the baghouse
dust auger and the slurry box to permit transport of treated baghouse fines
directly to the slurry box. A bulk concrete trailer was located near the
baghouse and a small auger was mounted between the slurry box and the
cement trailer to permit direct feed of cement to the slurry box. Finally,
a metered water line was installed to the slurry box and a flash mixer was
CanonteEnvircnmenta:
-------
mounted inside the slurry box to permit complete mixing of water, baghouse
dust, and cement.
With these modifications in place during the full-scale aeration, excavated
soil was fed to one of three hoppers in a hopper trailer. The soil was fed
onto a loading conveyor which transported the soil to the inlet end of the
materials dryer. The soil was discharged from the dryer to the bucket
elevator and then dropped through the recycle chute to the inlet end of the
dryer. A control gate in the chute directed the treated soil into the
materials dryer for further treatment or to an additional chute for
discharge to the concrete mixer truck. Baghouse fines, recycled to the
materials dryer during the pilot testing, were directed to the slurry box.
For each three-cubic yard volume, or "run", of soil processed, cement and
water were added to the fines in the slurry box and thoroughly mixed. Just
prior to discharge of the treated soil into the concrete mixer truck, the
gate on the bottom of the slurry box was opened and the slurry was
discharged to the concrete mixer truck. Normally three runs were
aggregated in the concrete mixer truck to form one batch, totaling
approximately eight to nine cubic yards.
During pilot testing of the aeration of petroleum area soils, Canonie
observed a bluish smoke emanating from the exhaust aeration stream.
Canonie installed HEPA filters, to remove the fine, smoky particulate.
Canonie's report of January, 1987, entitled "Petroleum Area Soils
Characterization and Remediation Analysis", details the engineering design
considerations in implementing the HEPA filter system.
CanonieEnvironn
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1\_ i. -- L v.
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3.0 AIR MONITORING
An extensive air monitoring network was developed to assess the impact of
site activities on ambient air quality during the pilot study phase of the
remediation at the McKin site. A full description of the elements included
in the network is presented in the "Soil Aeration Pilot Study Report",
dated April, 1986.
During the full-scale aeration of soils following the pilot study, Canonie
continued to monitor ambient air quality using a network similar to that
used in the pilot study. Organic vapor concentrations were monitored at
the site boundary at five locations. Century Instruments organic vapor
analyzers (OVAs) at those locations generated signals for transmission to a
computer which stored the data and determined whether certain prescribed
emission levels had been exceeded. High volume particulate monitors were
located at several of the perimeter stations to monitor total suspended
particulates. Organic vapor emissions near the excavation and the aeration
equipment were monitored using an OVA connected to an electronic data
logger. Meteorological data was also collected and stored on an electronic
data logger. At the end of each day, the monitoring data was stored onto
disks and a report of each week's air monitoring data was compiled for U.S.
EPA. This data has been forwarded to U.S. EPA under separate cover,
pursuant to U.S. IPA instructions.
Canonie also continued periodic air monitoring at ten nearby residences,
using an OVA with attached electronic data logger. Data on the neighbor-
hood air monitoring was presented to U.S. EPA and MOEP, together with
information on the on-site air monitoring network. The standards were
never exceeded.
Real-time particulate monitors were deleted from the air monitoring network
after pilot testing because readings from those monitors failed to coincide
with the results of high volume particulate sampling, conducted as part of
CanonieEnvironmentai
-------
the U.S. EPA nationwide air quality particulate program. The elimination
of the real-time particulate monitors in the network was approved by U.S.
EPA.
At the conclusion of the pilot study, Canonie requested and received
permission to change the method for analyzing the carbon and Tenax tubes
used to assess ambient air quality at the site perimeter. Originally,
Canonie proposed to utilize a system developed by Century Instruments,
whereby special tubes used in the collection of the samples are thermally
desorbed and the desorption gas is analyzed by a Century 128 GC OVA.
Canonie discovered that the desorption method was unreliable, resulting in
inaccurate values being reported for the test period. Canonie determined
that the method of desorption accepted by the National Institute of Occupa-
tional Safety and Health involved carbon disulfide desorption. At
Canonie's request, U.S. EPA approved the use of this method for ambient air
monitoring at the McKin site. Results of the carbon and Tenax tube
sampling indicated that TCE, the principle VOC of interest at the site, was
present in the ambient air at levels ranging from less than 0.002 up to
0.01 parts per million (ppm), well below the 2 ppm established as a health-
based standard for the site.
All changes to the air monitoring system were tested against benchmark
conditions prior to implementation and determined to provide accurate
reporting and analysis of ambient air conditions at the site. Air moni-
toring during the pilot study and the full-scale processing of nearly
11,500 cubic yards of soil at the McKin site demonstrated that the aeration
system control equipment was fully capable of controlling emissions of
VOCs. Indeed, volatile organic emission levels were met throughout the
aeration program. The primary air quality standard for particulates,
150 micrograms per cubic meter, was exceeded three times during the pilot
study portion of the project. However, the previously described changes to
the materials handling system eliminated the source of emissions such that
more than 10,000 cubic yards of soil were processed at the site without
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further exceedances of the primary air quality standard for total suspended
particulates.
When petroleum area soil aeration was underway, Canonie changed the
analytical parameters for carbon tube analysis to benzene, toluene, xylene,
and ethylbenzene. These constituents represent the pertinent analytical
parameters in view of their presence in the oily soils being treated. All
tube analyses for these parameters resulted in non-detectable
concentrations.
At the direction of U.S. EPA and MDEP, Canonie conducted polycyclic
aromatic hydrocarbon (PAH) analysis of the gas and vapor emanating from the
carbon bed exhaust stream during the petroleum area soil aeration pilot
study. The procedures used to analyze the vapor and gas in the exhaust
stream were submitted to U.S. EPA and MDEP on February 23, 1987, and
results of that analysis were transmitted by Canonie on March 11, April 6,
and April 23, 1987. The PAH constituents were non-detectable in both the
gaseous and vapor phases, utilizing the best available technology for
sampling and identification of PAH constituents. The vapor condensate and
scrubber mist eliminator analysis is presented in Appendix A.
This report does not contain the volumnious air monitoring data reports
submitted on a weekly basis while any excavation and/or aeration activity
was underway at the site. These weekly transmittals include all air
quality data obtained with summary explanations and are complete reports.
Charcoal tube QA/QC data is included in analytical reports which contain
the charcoal tube analytical results. High-volume particulate sampling
QA/QC data was included when a calibration or audit was performed on a
high-volume sampler motor. Lastly, high-volume particulate sampler filter
weight audits were presented on an interim basis. All QA/QC data indicate
acceptable performance in the subject areas previously mentioned. All of
this data is available in the offices of the U.S. EPA.
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3.1 Contingency Actions
The air monitoring systems were employed at the site to assess whether
predetermined action levels of VOCs were surpassed during site remedial
activities. The action level recommended by the Centers for Disease
Control permits the presence of total VOCs in concentrations not to exceed
2 ppm above background levels for a period not to exceed 15 minutes.
Throughout the full-scale site remediation, this standard was met.
Contingency actions were developed and are explained in Canonie's "Soil
Aeration Pilot Study Plan" and "Health and Safety Plan" of October, 1985.
Because the VOC air quality standard was always met, contingency actions
were never required.
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4.0 EXCAVATION TECHNIQUES UTILIZED
Sections 4.1 and 4.2 below describe the excavation of soil containing VOCs
and petroleum products, respectively.
4.1 Excavation of Soils Containing VOCs
Soils containing VOCs were located at Areas l(b), 3, 4, 6, and 8 and the
lagoon area of the site. These soils were excavated according to Canonie's
July, 1986 excavation plan for soils containing VOCs and agency comments
and clarifications thereto. A large trick crane equipped with an enclosed
caisson bucket was used to excavate most of the soils in Areas 3 and 6. A
rubber-tired backhoe was used to excavate soils in selected locations in
Areas 3 and 6, as well as all designated soils in Areas l(b), 4, and 8, and
the lagoon area. The soils in the latter group were designated for
excavation by backhoe due to the presence of low concentrations of organic
constituents in relatively shallow soils. The use of the backhoe to
excavate these areas was approved by U.S. EPA and MDEP prior to implementa-
tion of the excavation program.
Approximately 15,000 cubic yards of clean soil in Area 3 and 1,000 cubic
yards of clean soil in Area 6 were excavated and stockpiled on-site to
access underlying soils requiring treatment. The three-stage removal of
the clean soils from Area 3 provided even working surfaces for the
excavation of Caisson Borings 1 through 158 at Elevation 290 mean sea level
(MSL), the excavation of Caisson Borings 159 through 333 at Elevation 270
MSL, and the excavation of Caisson Borings 334 through 518 at Elevation 275
MSL. Removal of the clean soil excavated in Area 6 provided an even
working surface at Elevation 287.5 MSL. Upon completion of the excavation
and soil aeration in Areas 3 and 6, the clean, stockpiled soils were
returned to these areas by bulldozer, and the soils were compacted in one-
foot lifts to minimize long-term settlement.
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Figure 1 (the site map), maps the areas of excavation at the site on a
surveyed grid system. Figure 2 depicts the excavation and verification
sampling locations for Area l(b), Figures 3 and 4 indicate the excavation
area and verification sampling locations, respectively, for Area 3, Figure
5 shows the area of excavation and verification sampling locations for Area
4, Figures 6 and 7 indicate the excavation area and verification sampling
locations, respectively, for Area 6, and Figure 8 indicates the excavation
area and verification sampling locations for Area 8. A summary of the
excavation and treatment data for Areas 3 and 6 is presented in Table 1.
The summary of the excavation and treatment data for Areas l(b), 4, and 8
is listed in Table 2. Table 3 tabularizes excavation verification sample
locations with the respective TCE concentrations, and Table 4 lists the
results of the other analytes for these samples. The following highlights
the excavation of Areas l(b), 3, 4, 6, and 8. All excavation was based on
site characterization conducted to determine the areas requiring soil
treatment.
Area Hb)
Canonie excavated with a backhoe and treated approximately 605 cubic yards
of soil in this area. The excavation began at Elevation 298 MSL and ended
at Elevation 282 MSL.
Area 3
Canonie excavated and treated approximately 5,290 cubic yards of soil in
this area. Approximately 5,084 cubic yards of soil were excavated using
the caisson bucket, the remaining 206 cubic yards of soil were excavated
using a backhoe. The areas that were excavated using a backhoe are
described as follows:
1. The area having a center at construction coordinates N10, SE120
was excavated from Elevation 285 MSL to Elevation 275 MSL.
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2. The soil west of Caisson Borings 35 and 61 was excavated from
Elevation 287 MSL to Elevation 277 MSL.
3. The soil located at construction coordinates N 109, E 124 was
excavated from Elevation 285 MSL to Elevation 275 MSL.
4. The soil north of Caisson Borings 129 and 135 was excavated from
Elevation 285 MSL to Elevation 275 MSL.
5. The area having a center at construction coordinates N 127, E 108
was excavated from Elevation 270 MSL to Elevation 260 MSL.
Area 4
Canonie excavated with a backhoe and treated approximately 530 cubic yards
of material in this area. The depth of excavation, which began at Eleva-
tion 291 MSL, was approximately 11.0 feet, except for an area west of Soil
Boring SB4-6 that extended to 5.0 feet west of Soil Boring SB4-1, which was
excavated to a depth of 16.0 feet.
Area 6
Canonie excavated and treated approximately 1,731 cubic yards of soil in
this area. The caisson bucket was used to excavate the soil with the
exception of six cubic yards that were excavated using a backhoe. The soil
that was excavated using a backhoe was excavated from Elevation 287.5 MSL
to Elevation 277.5 MSL.
Area 8
Using a backhoe, Canonie excavated and treated approximately 1,250 cubic
yards of soil in this area. The depth of excavation, which began at Eleva-
tion 290 MSL, varied from 15 feet to 18 feet, then sloped in toward origi-
nal Soil Boring SB 8-20 to a depth of 21 feet.
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Lagoon
Canonie excavated with a backhoe and treated approximately 150 cubic yards
of soil in this area during the Soil Aeration Pilot Study. The actual
dates of excavation were May 22, 1986 through May 29, 1986. The excavation
began at Elevation 286.5 MSL and stopped at Elevation 276.5 MSL.
4.2 Excavation of Soils Containing Petroleum
Soils containing petroleum residues were located at Areas l(a), l(c), 2 and
9 of the site. Three of these areas (la), l(c), and 2 were characterized
in a subsurface profile, drilling, sampling, and analytical program
conducted in spring of 1986. The results of this program were summarized
in the report entitled "Petroleum Area Soils Characterization and
Remediation Analysis" dated January, 1987.
Canonie excavated Areas l(a), l(c), and 2 with a rubber-tired backhoe, in
accordance with U.S. EPA's letter to Canonie of November 26, 1986. The
excavation was initially conducted according to the visual extent of
petroleum substances, both in the vertical and horizontal planes.
Following a visual verification of the petroleum areas, a soil sampling and
analytical protocol was implemented to verify both the horizontal and
vertical perimeters of excavation. Based on these results, additional
soils were =>xcavated from Area 1, and the newly excavated perimeters were
re-verified.
Canonie completed the excavation of Areas l(a), l(c), and 2 on December 12,
1986. Figures 9 and 10 Indicate the areas of excavation for Petroleum
Areas l(a), l(c), and 2, respectively, and also indicate sampling loca-
tions. Table 5 indicates sampling elevations and Table 6 summarizes the
analytical results. The excavation, sampling, and analytical verification
were summarized in detail in a Canonie transmittal to U.S. EPA and MDEP on
March 16, 1987 entitled, "Excavation, Sampling, and Analytical Verification
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- Petroleum Areas l(a), l(c), and 2". This transmittal is included as
Appendix B.
Excavated material was delivered by backhoe to a screening plant. At the
screening plant, the soils and debris were separated on the screening deck,
with debris traveling over the deck to a waiting loader bucket. The debris
and separated soils were subsequently transported and stockpiled in two
separate locations, with berms and polyethylene covering provided to secure
the stockpiles.
Soils were also discovered and excavated from Area 9, which encompasses an
area adjacent to the old block incinerator building. Approximately 200
cubic yards of soil were removed and stockpiled from this area. The
petroleum residues present in these soils appeared to be relatively
unweathered compared to the petroleum residues present in the soils at
Areas l(a), l(c), and 2. Analysis of the petroleum residues from a
representative sample of these soils indicates no significant deviation
from the chemical characteristics of the residues found in Areas l(a),
l(c), and 2. Figure 11 depicts the Area 9 excavation and four perimeter
sampling locations, and Table 6 lists the analytical results of perimeter
samples.
Analysis of samples from sampling Location A9-4 initially revealed a
relatively high total extractable hydrocarbon concentration. Additional
soils were excavated from this area for use in the staging of petroleum
area soils required for processing. Figure 11 indicates the area of the
additional excavation.
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5.0 PROCESSING PARAMETERS
Sections 5.1 and 5.2 detail processing parameters required for the
successful remediation of soils containing VOCs and petroleum,
respectively.
5.1 Processing Parameters for Soils Containing VOCs
Soil containing VOCs in Areas l(b), 3, 4, 6, and 8 were excavated by
backhoe or by caisson auger and were placed into a rubber-tired front-end
loader with covered bucket for transport from the excavation area to the
aeration plant. The soils in the loader were discharged into one of three
staging hoppers. As processing required, soil staged in the hoppers was
released onto a conveyor belt, sifted through a coarse grate to remove
large rocks and boulders, and then discharged onto a second conveyor that
transported the soil to the feed hopper of the materials dryer. Aeration
of the soil was accomplished by forcing heated air through the length of
the dryer as the dryer rotated on its axis. As the soil traveled the
length of the dryer, soil temperatures rose to approximately 300 to 400
degrees Fahrenheit prior to discharge. The soil was discharged at the
burner end of the dryer onto a bucket elevator. The bucket elevator lifted
the soil to an overhead chute, which directed the soil from the bucket
elevator to the feed hopper of the materials dryer or the system discharge
chute.
The soil was typically cycled through the dryer three times. Each treated,
three-cubic-yard volume of soil constituted a "run". Three runs were
aggregated to create a "batch", the volume of which equalled the capacity
of the concrete truck used during full-scale soil processing. Soil
temperatures were maintained at 250 to 400 degrees Fahrenheit to optimize
volatilization. Air flow through the dryer was maintained at 15,000 actual
cubic feet per minute (acfm) to prevent excessive baghouse temperatures
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from developing. Stabilization was accomplished by adding cement and water
to each three-cubic-yard volume of soil for deposition into excavated
caisson holes.
5.2 Processing Parameters for Soils Containing Petroleum
When full aeration of soils containing petroleum was underway at Areas
l(a), l(c), 2, and 9, the soils were transported to a staging area located
west of the aeration plant. There, clean makeup soils were mixed with
petroleum area soils, using a front-end loader. The ratios of mixed soil
constituents were determined in the petroleum area pilot study primarily by
visual and physical inspection. The ideal soil mix contained the minimum
volume of clean soils required to produce a product that could be run
through the aeration system without agglomerating or "balling up". If the
soil mix were to agglomerate in the dryer, a flash fire could occur in the
dryer, with the potential to destroy the baghouse and remaining portions of
the aeration system. Table 7, which summarizes the processing of soils
containing petroleum, lists the volumes of clean, makeup soils required for
mixing.
Operational parameters used for processing the petroleum area soils were
consistent with the procedures detailed in Section 5.1 The addition of the
HEPA filter system required surveillance of the pressure drop across the
filters. This monitoring of the pressure drop across the filters was
accomplished using a manometer. New filters in the aeration system caused
a pressure drop of 1.5 Inches of water column. When the pressure drop
across the filters Increased to approximately 8.0 inches water column, a
filter change was necessary because breakthrough would occur at pressures
elevated above this level. During the first three weeks of petroleum area
soil aeration, the filters were changed approximately every two days.
However, during the final week of aeration, when unweathered Area 9 soils
were processed, the filters required changing twice daily, as the Area 9
soils produced a significantly heavier smoke stream that loaded the filters
more quickly.
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6.0 ANALYTICAL VERIFICATION
The areas of the site requiring treatment were verified through sampling
and analysis. Sections 6.1 and 6.2 discuss analytical methodologies to
address treated soils from the VOC-impacted areas and petroleum areas,
respectively. Section 6.3 describes the sampling and analytical
methodologies to address the excavated perimeters, and Section 6.4
discusses QA/QC documentation.
6.1 Analytical Verification of Treated Soils from VOC Areas
Canonie retrieved a sample of treated soil from each batch processed
through the aeration system originating from Areas l(b), 3, 4, 6, and 8.
Each sample was collected from the aerated soil mass as the soil was placed
into an excavated caisson or area of excavation. In general, the sample
was taken after half of the batch had been discharged. Under a
verification protocol approved by U.S. EPA, Canonie was required to test
half of the verification samples collected each day. When the average of
the samples tested resulted in a mean residual concentration of less than
0.10 mg/kg TCE, as agreed with EPA, Canonie certified that soils processed
during that day were appropriately treated. If the average of the samples
tested exceeded 0.10 mg/kg TCE, the remaining half of the samples were
analyzed, and the results of that analysis were included in the calculation
of the mean residual concentration. If the revised average resulted in a
mean residual concentration of less than 0.10 mg/kg TCE, the soils were
certified as being appropriately treated for the day. If the average of
the samples tested exceeded 0.10 mg/kg TCE, Canonie reprocessed the entire
volume of soil processed on that day. This occurred only once, on
January 9, 1987. Investigation of the processing plant on that day
indicated that a portion of the baghouse dust transfer chute was plugged
with roots and debris, thereby inhibiting the treatment of the dust at that
location. Cleaning of the transfer chute eliminated the problem.
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Canonie installed a fully configured gas chromatograph (GC) on-site in
order to obtain analytical results quickly and minimize downtime due to
delays in the return of analytical results. The GC was configured to
permit analysis of soil samples in accordance with U.S. EPA Methods 8010
and 8020. However, Canonie was required to analyze for only a limited
subset of constituents designated in the two methodologies. Canonie
normally analyzed the treated samples for the following compounds: benzene;
1,2-dichlorobenzene; 1,3-dichlorobenzene; 1,4-dichlorobenzene;
ethylbenzene; trans-l,2-dichloroethane; tetrachloroethylene; toluene;
1,1,1-trichloroethane; trichloroethylene; and xylenes. Approximately
10 percent of the samples analyzed on-site were sent to Canonie's Stockton
laboratory for confirmatory analysis.
The analytical results of treated soil samples were attached to soils
tracking logs assembled on a daily basis. The soils tracking logs, analyt-
ical tracking sheets, and sample chain-of-custody forms were transmitted to
U.S. EPA and MDEP periodically. The soils tracking logs indicate the traf-
fic flow of soils from excavation to treatment to redeposition. The daily
average of TCE in treated soil samples is indicated on the soils tracking
logs. A summary of this data is shown in Table 1, indicating location of
caisson excavation, elevations excavated, date of excavation, post-
treatment daily average TCE concentration, and the daily production volume
with which the treatment criteria was applied. Table 2 indicates the
pertinent data for excavation and treatment of areas excavated with a
backhoe.
6.2 Analytical Verification of Treated Soils from Petroleum Areas
The treated petroleum area soils originating from Areas l(a), l(c), 2, and
9 were sampled in the same manner as the soils described in Section 6.1.
Fifty percent of the samples were analyzed on-site for U.S. EPA 8010/8020
and at least 10 percent of the samples were analyzed off-site for poly-
cyclic aromatic hydrocarbons (PAHs) by U.S. EPA Method 8270 and total
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extractable hydrocarbons (TEH). The 8010/8020 analytical results for
treated soils (already transmitted to U.S. EPA and MDEP) do not indicate
the presence of detectable levels of aromatic compounds that were
originally present in the oily soils. The detection limit for these
constituents is 1 ppm. The 8010/8020 analytical results are not tabulated
in this report since the aromatic compounds are all non-detectable in post-
treatment samples. The Method 8270 and TEH analytical reports are
presented in Appendix C, with a daily summary of results given in Table 8.
The U.S. EPA and MDEP set certain treatment performance standards for the
aeration of the petroleum area soils. The treatment criteria specified
that not more than 1 ppm of each Method 8020 analyte (aromatic organics)
exist in treated soils with a 50 percent analytical frequency.
U.S. EPA and MDEP further specified that not more than 1 ppm of each PAH
constituent and not more than 10 ppm total PAH constituents detected in
Method 8270, exist in treated soils with a 10 percent analytical frequency.
Based upon treatment of all petroleum area soils, these criteria have been
satisfied as detailed in Section 7.2.
6.3 Analytical Verification of Excavated Areas
Canonie excavated all VOC-impacted soils according to the approved Excava-
tion Plan of July, 1986. All soils containing a TCE concentration in
excess of 1 ppm TCE were excavated and successfully aerated. In caisson
excavated Areas 3 and 6, a soil sample from each borehole located on or
outside of the 1 ppm TCE contour line was obtained at the elevation where
the most prevalent loading of volatile organics occurred. The locations of
these sampling verification points for Areas 3 and 6 are shown on Figures 4
and 7. Additional boreholes were excavated and treated beyond the 1.0 ppm
TCE contour if a sample indicated a TCE concentration greater than 1.0 ppm.
The additional boreholes were also analyzed to insure that any soil con-
taining TCE in concentrations greater than 1.0 ppm was excavated and
treated. The final perimeter samples with corresponding TCE concentrations
are listed in Table 3.
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The perimeter of Areas l(b), 4, and 8 were excavated using a backhoe and
were sampled in a manner stipulated by U.S. EPA and MDEP in a letter to
Canonie dated October 8, 1986. A complete list of all constituents
analyzed with their respective concentrations for VOC area excavation
perimeter samples is presented in Table 4.
The perimeter of petroleum Areas l(a), l(c), 2, and 9 (the petroleum areas)
were sampled in a manner specified by U.S. EPA and MDEP in a letter to
Canonie dated November 26, 1986. A complete list of all constituents
analyzed with their respective concentrations for petroleum area excavation
perimeter samples is present«d in Table 6.
6.4 QA/QC Documentation
Both Canonie's Stockton, CA analytical laboratory and the McKin on-site
laboratory participated in U.S. EPA's national proficiency sample program.
As part of additional QA/QC documentation, U.S. EPA required that Canonie
ship the extract of samples on-site to be tested for a qualitative
comparison in Canonie's Stockton, California analytical laboratory. The
comparison is presented in Appendix D and indicates that the analytes of
Methods 8010/8020 have been properly identified. In review of all existing
QA/QC documentation, Canonie validates the analytical data presented herein
as being accurate and precise.
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7.0 REMEDIATION OF SOILS
This section discusses the attainment of performance criteria for the
remedial activities conducted at the site. Section 7.1 discusses the
remediation of VOC-impacted Areas l(b), 3, 4, 6, and 8, and Section 7.2
discusses the successful remediation of Petroleum Areas l(a), l(c), 2, and
9. Section 7.3 reviews the ground water modeling support of the
performance standards used in remediation.
7.1 Remediation of Soils Containing VOCs
Based on the review of perimeter samples of the excavation of Areas l(b),
3, 4, 6 and 8, and the review of analytical results of treated soils exca-
vated from these areas, Canonie certifies that the soils impacted by VOCs
have been remediated to levels established by U.S. EPA and MDEP in the ROD
and subsequent correspondence as protective of public health, welfare, and
the environment.
The excavated and aerated soils from these areas satisfy the soil
performance standards specified in the McKin Record of Decision. All soils
that were excavated and aerated meet the 0.1 ppm TCE performance standard,
based on daily production volumes. A comparison of pre-treatment and post-
treatment samples indicating the successful removal of TCE as well as other
constituents is presented in Appendix E. Based on extensive analytical
data accumulated at the site, the TCE performance standard was demonstrated
to be extremely conservative in satisfying the ground water performance
standard applicable to water leaving the site perimeter as discussed in
Section 7.3. Canonie demonstrated in the Excavation Plan response to
comments of September, 1986, that a concentration of 1.0 ppm TCE can be
left remaining in site soils and amply meet the ground water performance
criteria.
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A review to verify the removal of VOCs other than TCE revealed that these
chemicals have been completely removed utilizing the low-temperature
thermal aeration except for a minimal number of instances where other
VOCs, such as dichlorobenzene or tetrachloroethene, were detected at
concentrations barely over detection limits.
A review of excavation perimeter sampling analysis indicates a few
instances where low residual concentrations of VOCs, such as xylene or
ethylbenzene, have been left remaining at the excavation perimeter. How-
ever, at these concentrations, the remaining residual constituents will not
adversely impact the ground water, since estimated ground water impact
levels would be orders of magnitude below any established or recommended
maximum contaminant limits for drinking water.
7.2 Remediation of Petroleum Areas
Based on the review of perimeter samples of the excavation of Areas l(a),
l(c), 2, and 9, and the review of analytical results of treated soils
excavated from these areas, Canonie certifies that the soils that have been
impacted by petroleum products have been remediated to levels established
by U.S. EPA and MDEP as protective of public health, welfare, and the
environment.
As discussed in Section 6.2, U.S. EPA and MDEP set certain treatment
performance standards for the removal of Method 8020 analytes from the
petroleum area soils. The Method 8020 analytes were removed completely to
non-detection during the petroleum area soil aeration.
Polycyclic Aromatic Hydrocarbon (PAH) constituents were removed to levels
which meet the performance criteria specified by U.S. EPA and MDEP. The
results of pre-treatment and post-treatment sampling of petroleum area
soils for these and other constituents is included in Appendix F. The
results of PAH and TEH analysis over the duration of petroleum area soil
aeration are summarized in Table 8. The frequency of the sampling and
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analysis of treated batches for PAH constituents was 10 percent. During
the last two weeks of petroleum area soil aeration, one PAH constituent,
phenanthrene, was detected in a number of treated samples above 1 ppm.
However, for the duration of petroleum area soil aeration, the average
concentration of phenanthrene was 0.92 ppm, below the performance standard.
Canonie summarized the Method 8270 analytical results and transmitted the
data to U.S. EPA and MDEP on April 27, 1987. Canonie demonstrated in that
report that the performance criteria should be applied to the project
duration, and U.S. EPA and MDEP accepted the results of petroleum area soil
aeration and approved backfilling of treated soil on April 30, 1987. The
location of the backfilled, treated soils is illustrated on Figure 12.
No TEH standard was imposed because all chemical constituents were being
verified separately by U.S. EPA Methods 8010/8020 and 8270.
The final TEH average concentration for treated petroleum area soils is
approximately 110 ppm. Since the volatile and aromatic organic criteria
and PAH criteria have been satisfied, and the TEH residual concentrations
are well within projected limits, the petroleum area soils have been
remediated to levels established by U.S. EPA and MDEP. The system was able
to effectively treat soils impacted by petroleum products with the proper
mixing and staging of soils, as summarized in Table 7.
7.3 Hydrocarbon Fate and Ground Water Transport
The original remedial investigation and feasibility study for the McKin
site indicated that an analysis, using the SOCEM Model, requires treatment
of all soils excavated with a TCE concentration of 0.1 ppm. Upon conclu-
sion of the soil sampling and analysis phase of the site characterization
verification program, Canonie reviewed the input parameters utilized in the
original SOCEM model analysis. In accordance with an engineering analysis
of physical parameters of the site and its soils, and after a review of
available information on partitioning coefficients for TCE in soils,
Canonie issued a report on July 11, 1986 concluding that only excavation
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and treatment of soils containing a TCE concentration greater than 1.0 ppm
was required to meet the ground water remedial criteria developed for the
project. Several additional letter reports issued after the July 11, 1986
report clarified the engineering analysis completed by Canonie and present-
ed the technical reports on research conducted by Stanford University on
partitioning coefficients.
Based upon review of the reports, U.S. EPA approved the Excavation Plan
submitted by Canonie. The treated and stabilized soils will restrict
ground water movement and prevent infiltration, and the regrading and
landscaping of the site will reduce the amount of precipitation
infiltrating the site.
Concurrent with excavation of soils at the 1.0 ppm TCE contour, Canonie
sampled the soils to verify that the residual TCE level in the soil was
below the 1.0 ppm TCE criteria. Analysis of boreholes on the final perime-
ter of each designated excavation area show that residual TCE levels in the
soil do not exceed the 1.0 mg/kg excavation standard. However, analytical
results from a few perimeter boreholes indicated the presence of detectable
levels of xylene and/or ethyl benzene. These compounds, while present in
some of the soils from Areas l(b), 3, 4, and 8, were not designated as
indicator organic constituents for the purpose of defining soils to be
excavated and treated. Analysis of constituent fate and transport of the
xylene and/or ethylbenzene residual in the perimeter borehole soils, using
the SOCEM model and corresponding Input parameters, confirms that the pre-
dicted impact of ground water quality from the residual will not exceed any
mandated or recommended drinking water standard.
Upon completion of the aeration of soil from Areas l(b), 3, 4, 6, and 8,
Canonie excavated and stockpiled soils from Areas l(a), l(c), 2, and 9.
Canonie developed an excavation and treatment plan for these soils based
upon published data relating to the mobility and partitioning of xylenes.
Canonie anticipated that a treatment level of 1 mg/kg could be achieved in
the aeration system. Therefore, Canonie analyzed the predicted impact to
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ground water from a residual xylene concentration of 1 mg/kg. Xylenes were
selected as the indicator compounds since xylenes were the most prevalent
compounds and were the most mobile of petroleum hydrocarbons present in the
petroleum area soils.
Analysis using the SOCEM model and appropriate input parameters indicated
that the presence of 1 mg/kg of any hydrocarbon constituent in the
untreated petroleum area soils will not result in an impact which will
exceed mandated or recommended drinking water criteria at any location on
the site. Post excavation sampling of Areas l(a), l(c), 2, and 9 indicated
residual xylene concentrations of less than 1.0 mg/kg. Post-aeration
analysis routinely reported residual xylene concentrations of less than
1.0 mg/kg.
CanonieEnvironmenta!
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25
8.0 SUBSEQUENT ON-SITE ACTIONS FOR PROTECTION
OF PUBLIC HEALTH, WELFARE, AND ENVIRONMENT
Canonie has considered whether subsequent on-site actions are necessary to
protect public health, welfare, and the environment from any release or
threat of a release of hazardous substances from soils at the site.
Because all soils known to contain chemical constituents exceeding U.S. EPA
and MDEP soil performance standards have been removed and treated to levels
established by U.S. EPA and MDEP, further on-site actions are not required.
CanonieEnvironn
itrl .L
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26
9.0 SITE DEMOBILIZATION AND CLOSURE
Upon authorization from U.S. EPA and MDEP, the aeration system and all
associated equipment were dismantled and decontaminated according to
Canonie's letters to U.S. EPA and MDEP titled "Demobilization and Site
Closure Activities" and "Decontamination and Disposition of Equipment"
dated April 17, and May 6, 1987, respectively. These activities were
conducted in accordance with decontamination procedures specified in
Canonie's Closure Action Work Plan (CAP) dated October, 1985 and approved
by the agencies.
Generally, each item to be decontaminated was transported to the decon-
tamination pad where the item was triple washed with a soapy hot water,
high pressure solution. The item was then inspected based on the decon-
tamination certification criteria listed in the CAP. These criteria
include visual absence of foreign substances, films, or colors and an
organic vapor analyzer (OVA) screen to ensure no sources of organic vapor
evolution are present. All items were properly certified as decontaminated
according to the procedures, under the direction of a licensed professional
engineer in the state of Maine, Mr. Timothy J. Harrington. Mr.
Harrington's signed certification of the proper decontamination of items is
included in Appendix G.
The decontamination rinseate solution was collected in the sump and pumped
to a holding tank. Approximately 1,500 gallons were collected. The rinse-
ate was treated with the carbon unit on-site and then sampled and analyzed.
Due to a phenol concentration of approximately 2 ppm in the analyzed rinse-
ate, the solution was incinerated at Trade Waste Incineration (TWI) for
final disposal. Any other accumulated solids or sludges from the
decontamination process were placed in the oily debris stockpile for final
disposal at Chemical Waste Management, Emelle, Alabama.
CanonieEnvironmerlai
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27
The final disposition of equipment was accomplished according to the docu-
ments previously referenced in this section. The aeration system was
decontaminated and transported off-site on May 15, 1987. Items which were
decontaminated, certified, and backfilled on-site were deposited in the
area of the former lagoon. This area is shown on Figure 13.
Site grading was completed, using a D-7 bulldozer, on May 8, 1987. A
topographic map illustrating site elevation contours was transmitted to
U.S. EPA and MDEP on May 14, 1987, and is shown on Figure 14. A sample of
loam material and list of constituents in the seed mixture to be used for
learning and seeding were submitted to U.S. EPA and MDEP and approval was
received for their subsequent use at the end of May, 1987. The spreading
of the sandy loam to a uniform depth of four inches was completed on
June 12, 1987, and hydroseeding was completed on June 17, 1987. The rela-
tively flat (4:1) slopes and the use of a stable loam mixture and proper
grass seeding will ensure that erosion-resistant conditions exist.
The remaining site closure items were completed on June 23, 1986. At that
time, all drums and bulk oily debris were transported for off-site dis-
posal. Additionally, the site has been loamed and seeded, and the remain-
ing site trailer and equipment have been removed. The remaining items
inside the perimeter fence include the decontamination pad and the buried
septic tank.
All items presented in the original CAP have been completed. The area of
buried drums, which was excavated and drums subsequently disposed, was
addressed in a letter and transmittal of analytical results on July 2,
1986. The underground fuel oil tank was properly decommissioned,
excavated, decontaminated, and reburied in the old lagoon area. The
analytical results indicating non-detection of PCBs in the soils underlying
the fuel oil tank is included in Appendix A.
CanonieE
nvronme
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28
10.0 OFF-SITE DISPOSAL OF ACCUMULATED MATERIALS
During work conducted under the original Administrative Order, a number of
different waste materials were accumulated for off-site disposal. These
materials Include the following:
1. Two hundred and eighty drums of oily sludge were Incinerated at
Trade Waste Incineration (TWI) of Sauget, Illinois, a subsidiary
of Chemical Waste Management.
2. One hundred and twenty drums of cut rubber hose were incinerated
at SCA Chemical Services (SCA) of Chicago, Illinois, a subsidiary
of Chemical Waste Management.
3. Thirteen excavated drums with residual waste oil were incinerated
at TWI.
4. Twelve drums of asbestos were disposed at Chemical Waste
Management of Emelle, Alabama.
5. Six hundred and sixty gallons of waste fuel oil and tank rinseate
were incinerated at SCA.
The completed manifest forms for these materials are Included in Appen-
dix H. The manifest forms for Items 1 and 5 were completed to Chemical
Waste Management of Model City, New York, where they were temporarily
stored before their ultimate disposal. Canonie will transmit the completed
forms indicating the transfer from Model City, New York to the disposal
facility.
During work conducted following the original Administrative Order, addi-
tional wastes were accumulated for off-site disposal. These materials are
as follows:
CanonieEnvironmerital
-------
29
1. Three hundred cubic yards of oily debris were disposed at Chemical
Waste Management of Emelle, Alabama.
2. Thirty-eight drums of spent HEPA filters were incinerated at TWI.
3. Twenty-nine drums of spent baghouse bags were incinerated at TWI.
4. Forty-two drums of used Tyveks, etc. were incinerated at TWI.
5. Fourteen drums of cut rubber hose were incinerated at TWI.
6. One thousand five hundred gallons of waste oil/water were
incinerated at TWI.
The signed manifests from the site are included in Appendix H. The com-
pleted forms signed from the disposal facility will be forwarded to U.S.
EPA and MDEP upon receipt.
In addition to the materials previously mentioned, spent vapor phase carbon
used in the aeration treatment system was regenerated at Calgon Carbon
Corporation's (Calgon's) reactivation facilities in Neville Island,
Pennsylvania, and Columbus, Ohio. In October, 1986, approximately 30,000
pounds of carbon were reactivated, and in April, 1987, approximately 15,000
pounds of carbon were transported for reactivation. Calgon's letter
indicating receipt of the carbon is included in Appendix H. The carbon
analysis for total chlorinated compounds has never revealed such compounds
in concentrations exceeding 1.0 percent. The 1,000 pounds of carbon used
in the treatment of scrubber liquid was reactivated in May, 1987, by
Adsorption Systems, Inc., of Mi 11 burn, New Jersey.
CanonieEnvironmentai
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30
11.0 COST BREAKDOWN FOR AERATION OF SOILS
A summary of costs incurred for the aeration of soils excavated from Areas
l(b), 3, 4, 6, and 8 is included in Table 9. A summary of costs incurred
for the aeration of petroleum area soils excavated from Areas l(a), l(c),
2, and 9 is included in Table 10.
CanonieEnvironmenta!
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31
12.0 SUMMARY
In conclusion, the following actions have been completed in the remediation
of the McKin Superfund site:
1. Complete characterization of site soils to determine the extent of
soils impacted and extent of remediation required, as summarized
in Table 11;
2. Development of a process to aerate impacted soils while meeting
site-specific air quality standards;
3. Treatment of impacted soils to concentrations within specified
performance limits;
4. Verification of remaining soils using a ground water model to
demonstrate that ground water performance criteria are satisfied
as specified in the Record of Decision;
5. Remediation of three petroleum areas on-site utilizing the devel-
oped technology;
6. Completion of site closure activities as required in the Record of
Decision and approved work plans.
Respectfully submitted,
~
Brian M. Bell
Project Engineer
hillip E. Antommaria
Executive Vice President
BMB/PEA/pr
CanonieEnvircnmenta!
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REFERENCES
1. Canonie Engineers, Inc., "Soil Aeration Pilot Study", report submitted
to U.S. Environmental Protection Agency and Maine Department of
Environmental Protection, April, 1986.
2. Canonie Environmental Services Corp., "Petroleum Area Soils
Characterization and Remediation Analysis", report submitted to U.S.
Environmental Protection Agency and Maine Department of Environmental
Protection, January, 1987.
3. Canonie Environmental Services Corp., "Air Monitoring Reports,
Petroleum Area Soil Aeration Pilot Study", report submitted to U.S.
Environmental Protection Agency and Maine Department of Environmental
Protection, March !\ April 6, and April 23, 1987.
4. Canonie Engineers, Inc., "Excavation Plan", report submitted to U.S.
Environmental Protection Agency and Maine Department of Environmental
Protection, July 11, 1986.
5. Canonie Engineers, Inc., "Soil Aeration Pilot Study Plan", report
submitted to U.S. Environmental Protection Agency and Maine Department
of Environmental Protection, October, 1985.
6. Canonie Engineers, Inc., "Health and Safety Plan", report submitted to
U.S. Environmental Protection Agency and Maine Department of
Environmental Protection, October, 1985.
7. Canonie Engineers, Inc., "Excavation, Sampling, and Analytical
Verification - Petroleum Areas l(a), l(c), and 2", submitted to U.S.
Environmental Protection Agency and Maine Department of Environmental
Protection, March 16, 1987.
8. Canonie Environmental Services Corp., "Excavation Plan Response to
Comments", report submitted to U.S. Environmental Protection Agency
and Maine Department of Environmental Protection, September, 1986.
9. Canonie Environmental Services Corp., "Summary of GC/MS Analytical
Data, Aeration of Petroleum Area Soils", submitted to U.S.
Environmental Protection Agency and Maine Department of Environmental
Protection, April 27, 1987.
10. Canonie Environmental Services Corp., "Demobilization and Site Closure
Activities", submitted to U.S. Environmental Protection Agency and
Maine Department of Environmental Protection, April 17, 1987.
11. Canonie Environmental Services Corp., "Decontamination and Disposition
of Equipment", submitted to U.S. Environmental Protection Agency and
Maine Department of Environmental Protection, May 6, 1987.
CanonieEnvironmental
-------
REFERENCES
(Continued)
12. Canonie Engineers, Inc., "Closure Action Work Plan", submitted to U.S.
Environmental Protection Agency and Maine Department of Environmental
Protection, October, 1985.
13. Canonie Engineers, Inc., "Transmittal of Analytical Results, Drum Area
Excavation and Analysis", submitted to U.S. Environmental Protection
Agency and Maine Department of Environmental Protection, July 2, 1986.
CanonieEnvircnmental
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TABLE 1
SUMMARY OF EXCAVATION AND TREATMENT DATA
AREAS 3 AND 6
Area-
Caisson
Boring
Treated Soil
Beginning
Number Location Elevation
3-1
3-2
3-3
3-4
3-5
3-6
3-7
3-8
3-9
3-10
3-11
3-12
3-13
3-14
3-15
3-16
3-17
3-18
3-19
3-20
3-21
3-22
3-23
3-24
3-25
3-26
3-27
3-28
3-29
3-30
3-31
3-32
3-33
3-34
3-35
3-36
3-37
3-38
3-39
N115
N115
N115
N115
N115
N115
N115
N115
N113
N113
N114
N114
N114
N115
N114
N115
N114
N114
N113
N114
N113
N113
N115
N114
N113
N113
N113
N112
N114
N112
N112
N112
N112
N114
N112
N112
N112
N112
Nlll
E126
E130
E122
E118
E124
E128
E132
E120
E130
E118
E123
E131
E119
E116
E125
E134
E129
E121
E124
E133
E128
E120
E136
E127
E132
E122
E126
E129
E117
E119
E131
E123
E127
E135
E117
E125
E133
E121
E114
290
290
290
290
290
290
290
290
290
290
290
290
290
290
290
290
290
290
290
290
290
290
290
290
290
290
290
290
290
290
290
290
290
290
290
290
290
290
290
Ending
Elevation
258
258
258
258
258
258
248
258
258
258
258
254
258
258
258
248
258
258
258
248
258
258
248
258
252
258
258
258
258
261
261
261
261
261
264
261
261
261
265
Date
Excavated
02-17-86
02-25-86
03-05-86
03-10-86
03-17-86
03-20-86
03-21-86
03-21-86
03-21-86
03-22-86
03-22-86
03-24-86
03-25-86
03-25-86
03-25-86
03-26-86
03-26-86
03-26-86
03-27-86
03-28-86
03-28-86
03-28-86
03-28-86
03-31-86
03-31-86
03-31-86
04-01-86
04-02-86
04-02-86
04-02-86
04-03-86
04-03-86
04-03-86
04-03-86
04-04-86
04-04-86
05-14-86
05-15-86
05-20-86
Post-
Treatment
Daily Avg.
TCE Cone.
(ppm)
*
NO 0.02
*
ND 0.02
ND 0.05
ND 0.05
< 0.052
< 0.055
< 0.05
< 0.058
< 0.051
ND 0.05
< 0.05
< 0.066
< 0.058
< 0.056
ND 0.05
ND 0.05
ND 0.05
ND 0.02
ND 0.02
Daily
Treated
Volume
(cu. yds)
19
19
19
19
19
19
62
38
21
57
62
19
87
60
19
55
68
32
17
17
15
*Soil was processed during the soil aeration pilot study.
CanonieEnvironmerldi
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TABLE 1
SUMMARY OF EXCAVATION AND TREATMENT DATA
AREAS 3 AND 6
(Continued)
Area-
Caisson
Boring
Number
3-40
3-41
3-42
3-43
3-44
3-45
3-46
3-47
3-48
3-49
3-50
3-51
3-52
3-53
3-54
3-55
3-56
3-57
3-58
3-59
3-60
3-61
3-62
3-63
3-64
3-65
3-66
3-67
3-68
3-69
3-70
3-71
3-72
3-73
3-74
3-75
3-76
3-77
3-78
3-79
3-80
Location
N113
Nlll
Nlll
Nlll
Nlll
Nlll
N112
Nlll
Nlll
Nlll
Nlll
N116
N116
N116
N116
N116
N116
N116
N116
N116
N116
N114
N117
N117
N117
N117
N117
N117
N117
N117
N117
N117
N118
N118
N118
N118
N118
N118
N118
N118
N119
E134
E132
E128
E124
E120
E116"
E135
E130
E126
E122
E118
E117
E121
E125
E129
E133
E115
E119
E123
E127
E131
E115
E116
E120
E124
E128
E132
E118
E122
E126
E130
E134
E117
E121
E125
E129
E133
E119
E123
E127
E118
Treated
Beginning
Elevation
290
290
290
290
290
290
290
290
290
290
290
290
290
290
290
290
290
290
290
290
290
290
290
290
290
290
290
290
290
290
290
290
290
290
290
290
290
290
290
290
290
Soil
Ending
Elevation
258
265
265
265
265
265
260
265
265
265
264
265
265
265
260
255
265
265
265
265
260
280
265
265
265
260
255
265
265
265
260
255
265
265
265
265
255
265
265
265
265
Date
Excavated
07-08-86
07-08-86
07-08-86
07-08-86
07-09-86
07-09-86
07-10-86
07-10-86
07-10-86
07-10-86
07-10-86
07-11-86
07-11-86
07-11-86
07-14-86
07-14-86
07-14-86
07-14-86
07-15-86
07-15-86
07-15-86
07-15-86
07-15-86
07-15-86
07-16-86
07-16-86
07-16-86
07-16-86
07-17-86
07-17-86
07-18-86
07-18-86
07-21-86
07-21-86
07-21-86
07-21-86
07-21-86
07-22-86
07-22-86
07-22-86
07-22-86
Post-
Treatment
Daily Avg.
TCE Cone.
(ppm)
ND 0.02
< 0.033
ND 0.02
< 0.03
< 0.03
< 0.025
ND 0.02
ND 0.02
ND 0.02
ND 0.02
ND 0.02
Daily
Treated
Volume
(cu. yds)
63
29
77
44
68
82
68
29
38
80
59
CanonieEnvironmenta 1
-------
TABLE 1
SUMMARY OF EXCAVATION AND TREATMENT DATA
AREAS 3 AND 6
(Continued)
Area-
Caisson
Boring
Number
3-81
3-82
3-83
3-84
3-85
3-86
3-87
3-88
3-89
3-90
3-91
3-92
3-93
3-94
3-95
3-96
3-97
3-98
3-99
3-100
3-101
3-102
3-103
3-104
3-105
3-106
3-107
3-108
3-109
3-110
3-111
3-112
3-113
3-114
3-115
3-116
3-117
3-118
3-119
3-120
3-121
Location
N119
N119
N119
N118
N119
N119
N119
N118
N119
N119
N119
N119
N119
N119
N119
N119
N119
N119
N119
N119
N120
N120
N120
N119
N120
N120
N120
N120
N120
N121
N121
N121
N120
N120
N121
N121
N121
N121
N121
N122
N122
E122
E126
E130
E131
E120
E124
E128
E135
E116
E122
E126
E130
E134
E120
E124
E128
E132
E130
E136
E128
E117
E121
E125
E132
E119
E123
E127
E131
E135
E118
E122
E126
E129
E133
E120
E124
E128
E132
E136
E119
E123
Treated
Beginning
Elevation
290
290
290
290
290
290
290
290
290
290
290
290
290
290
290
290
290
290
290
290
290
290
290
290
290
290
290
290
290
290
290
290
290
290
290
290
290
290
290
290
290
Soil
Ending
Elevation
265
265
260
255
265
265
265
255
280
265
265
260
255
265
265
265
260
260
255
265
280
265
265
260
260
265
265
260
260
280
265
260
260
260
280
265
260
260
260
280
280
Date
Excavated
07-23-86
07-23-86
07-23-86
07-25-86
07-26-86
07-26-86
07-26-86
07-26-86
07-26-86
07-26-86
07-28-86
07-28-86
07-28-86
07-28-86
07-29-86
07-29-86
07-29-86
07-29-86
07-29-86
07-30-86
07-30-86
07-30-86
07-30-86
07-31-86
07-31-86
07-31-86
07-31-86
07-31-86
07-31-86
07-31-86
08-01-86
08-01-86
08-01-86
08-01-86
08-01-86
08-01-86
08-04-86
08-04-86
08-04-86
08-04-86
08-04-86
Post-
Treatment
Daily Avg.
TCE Cone.
(ppm)
ND 0.02
ND 0.02
ND 0.02
< 0.041
ND 0.02
ND 0.02
ND 0.02
ND 0.02
Daily
Treated
Volume
(cu. yds)
47
21
85
68
85
50
103
ND 0.02
65
CanonieEnvironmentd
-------
TABLE 1
SUMMARY OF EXCAVATION AND TREATMENT DATA
AREAS 3 AND 6
(Continued)
Area-
Caisson
Boring
Number
3-122
3-123
3-124
3-125
3-126
3-127
3-128
3-129
3-130
3-131
3-132
3-133
3-134
3-135
3-136
3-137
3-138
3-139
3-140
3-141
3-142
3-143
3-144
3-145
3-146
3-147
3-148
3-149
3-150
3-151
3-152
3-153
3-154
3-155
3-156
3-157
3-158
6-1
Location
N122
N122
N122
N122
N122
N122
N122
N123
N118
N116
N123
N123
N123
N123
N123
N117
N121
N121
N110
N110
N110
N108
N108
N108
N110
N110
N110
N108
N108
N118
N116
N109
N109
N109
N109
N109
N117
N122
E127
E131
E135
E125
E121
E129
E133
E122
E133
E135
E132
E128
E124
E126
E130
E134
E131
E130
E119
E123
E127
E125
E121
E117
E125
E121
E117
E123
E119
E135
E137
E116
E120
E118
E122
E126
E136
E124
Treated
Beginning
Elevation
290
290
290
290
290
290
290
290
290
290
290
290
290
290
290
290
290
290
290
290
290
290
290
290
290
290
290
290
290
290
290
290
290
290
290
290
290
287.5
Soil
Ending
Elevation
260
260
260
265
280
260
260
280
255
255
260
260
280
280
260
255
260
260
265
265
265
265
275
275
265
265
275
265
275
255
255
275
265
275
265
265
255
261.5
Post-
Treatment Daily
Daily Avg. Treated
Date TCE Cone. Volume
Excavated (ppm) (cu. yds)
08-05-86
08-05-86
08-05-86
08-05-86
08-05-86
08-05-86 ND 0.02 91
08-06-86
08-06-86
08-06-86
08-06-86
08-06-86
08-06-86
08-06-86 ND 0.02 106
08-07-86
08-07-86
08-07-86 ND 0.02 44
08-08-86
08-08-86
08-08-86
08-08-86
08-08-86
08-08-86
08-08-86
08-08-86 ND 0.02 112
08-11-86
08-11-86
08-11-86
08-11-86
08-11-86
08-11-86
08-11-86
08-11-86
08-11-86 ND 0.02 127
08-12-86
08-12-86
08-12-86
08-12-86
08-12-86 ND 0.02 74
CanonieEnvironmentdi
-------
TABLE 1
SUMMARY OF EXCAVATION AND TREATMENT DATA
AREAS 3 AND 6
(Continued)
Area-
Caisson
Boring
Number Location
6-2 N122
6-3 N120
6-4 N120
6-5 N120
6-6 N122
6-7 N122
6-8 N120
6-9 N121
6-10 N121
6-11 N118
6-12 N118
6-13 N118
6-14 N118
6-15 N121
6-16 N121
6-17 N120
6-18 N118
6-19 N118
6-20 N121
6-21 N121
6-22 N119
6-23 N119
6-24 N119
6-25 N119
6-26 N119
6-27 N120
6-28 N120
6-29 N120
6-30 N117
6-31 N117
6-32 N117
6-33 N117
6-34 N117
6-35 N120
6-36 N119
6-37 N119
6-38 N119
6-39 N118
6-40 N117
6-41 N117
6-42 N117
E120
E128
E124
E118
E126
E122
E112
E127
E121
E128
E122
E118
E114
E125
E119
E114
E116
E120
E117
E123
E127
E113
E109
E119
Elll
E126
E122
E116
E127
E123
E119
E115
Elll
E120
E115
E121
E125
E106
E125
E121
E117
Treated
Beginning
Elevation
287.5
287.5
287.5
287.5
287.5
287.5
287.5
287.5
287.5
287.5
287.5
287.5
287.5
287.5
287.5
287.5
287.5
287.5
287.5
287.5
287.5
287.5
287.5
287.5
287.5
287.5
287.5
287.5
287.5
287.5
287.5
287.5
287.5
287.5
287.5
287.5
287.5
287.5
287.5
287.5
287.5
Soil
Ending
Elevation
265.5
267.5
266.5
267.5
265.5
262.5
266.5
268.5
265.5
269.5
267.5
266.5
266.5
264.5
266.5
266.5
266.5
266.5
274.5
261.5
266.5
266.5
267.5
266.5
267.5
265.5
277.5
276.5
282.5
281.5
267.5
267.5
267.5
269.5
267.5
269.5
279.5
274.5
279.5
267.5
267.5
Post-
Treatment Daily
Daily Avg. Treated
Date TCE Cone. Volume
Excavated (ppm) (cu. yds)
08-13-86
08-13-86
08-13-86 ND 0.02 37
08-15-86
08-15-86
08-15-86
08-15-86 ND 0.02 52
08-18-86
08-18-86
08-18-86
08-18-86
08-18-86
08-18-86 ND 0.02 71
08-20-86
08-20-86
08-20-86
08-20-86
08-20-86 ND 0.02 63
08-21-86
08-21-86
08-21-86
08-21-86
08-21-86
08-21-86 ND 0.02 72
08-22-86
08-22-86
08-22-86
08-22-86
08-22-86
08-22-86
08-22-86
08-22-86
08-22-86
08-22-86 ND 0.02 90
08-23-86
08-23-86
08-23-86
08-23-86
08-23-86
08-23-86
08-23-86
CanonieEnvircnmentd
-------
TABLE 1
SUMMARY OF EXCAVATION AND TREATMENT DATA
AREAS 3 AND 6
(Continued)
Area-
Caisson
Boring
Number
6-43
6-44
6-45
6-46
6-47
6-48
6-49
6-50
6-51
6-52
6-53
6-54
6-55
6-56
6-57
6-58
6-59
6-60
6-61
6-62
6-63
6-64
6-65
6-66
6-67
6-68
6-69
6-70
6-71
6-72
6-73
6-74
6-75
6-76
6-77
6-78
Location
N117
N117
N117
N119
N118
N119
N118
N118
N118
N116
N118
N116
N116
N116
N116
N114
N114
N116
N116
N117
N116
N116
N116
N115
N115
N114
N115
N115
N115
N114
N115
N115
N115
N113
N115
N113
N113
E113
E109
E105
E123
E126
E117
E124
E112
E108
E124
E110
E120
E116
E112
E108
E122
E118
E118
E106
£107
E110
E114
E122
E126
E119
E106
E123
£115
£111
£120
£121
£117
£113
£121
£109
£117
£113
Treated
Beginning
Elevation
287.5
287.5
287.5
287.5
287.5
287.5
287.5
287.5
287.5
287.5
287.5
287.5
287.5
287.5
287.5
287.5
287.5
287.5
287.5
287.5
287.5
287.5
287.5
287.5
287.5
287.5
287.5
287.5
287.5
287.5
287.5
287.5
287.5
287.5
287.5
287.5
287.5
Soil
Ending
Elevation
266.5
266.5
267.5
274.5
279.5
265.5
279.5
267.5
267.5
279.5
267.5
267.5
267.5
266.5
265.5
266.5
267.5
267.5
266.5
266.5
268.5
266.5
267.5
267.5
267.5
266.5
267.5
267.5
266.5
267.5
267.5
267.5
267.5
267.5
267.5
267.5
267.5
Post-
Treatment
Daily Avg.
Date TCE Cone.
Excavated (ppm)
08-23-86
08-23-86 ND 0.07
08-25-86
08-25-86
08-25-86
08-25-86
08-25-86
08-25-86 ND 0.02
08-27-86
08-27-86 ND 0.02
08-28-86
08-28-86
08-28-86
08-28-86
08-28-86
08-28-86
08-28-86
08-28-86 ND 0.02
08-29-86
08-29-86
08-29-86
08-29-86
08-29-86
08-29-86
08-29-86
08-29-86 ND 0.02
09-02-86
09-02-86
09-02-86
09-02-86 ND 0.02
09-03-86
09-03-86
09-03-86
09-03-86
09-03-86
09-03-86
09-03-86 ND 0.02
Daily
Treated
Volume
(cu. yds)
87
54
17
97
96
48
82
CanonieEnvironmer.tc
-------
TABLE 1
SUMMARY OF EXCAVATION AND TREATMENT DATA
AREAS 3 AND 6
(Continued)
Area-
Caisson
Boring
Number
3-159
3-160
3-161
3-162
3-163
3-164
3-165
3-166
3-167
3-168
3-169
3-170
3-171
3-172
3-173
3-174
3-175
3-176
3-177
3-178
3-179
3-180
3-181
3-182
3-183
3-184
3-185
3-186
3-187
3-188
3-189
3-190
3-191
3-192
3-193
3-194
3-195
3-196
3-197
3-198
3-199
3-200
3-201
Location
N134
N134
N134
N134
N134
N132
N132
N132
N134
N134
N134
N134
N134
N132
N132
N132
N132
N133
N133
N133
N133
N133
N131
N131
N131
N133
N133
N133
N133
N133
N133
N131
N131
N131
N135
N135
N135
N135
N131
N131
N131
N131
N131
E161
E157
E153
E149
E145
E161
E157
E153
E159
E155
E151
E147
1143
E159
E155
E151
E147
E144
E148
E152
E156
E160
E162
E154
E150
E162
E158
E154
E150
E146
E142
E140
E144
E148
E148
E152
E156
E160
E160
E156
E152
E146
E142
Treated
Beginning
Elevation
260
260
260
260
260
260
260
260
260
260
260
260
260
260
260
260
260
260
260
260
260
260
260
260
260
260
260
260
260
260
260
260
260
260
260
260
260
260
260
260
260
260
260
Soil
Ending
Elevation
250
246
246
250
250
250
25U
250
245
246
250
250
250
250
250
250
250
250
250
250
245
250
250
250
250
250
250
250
250
250
250
250
250
250
250
245
245
245
250
250
250
250
250
Post-
Treatment Daily
Daily Avg. Treated
Date TCE Cone. Volume
Excavated (ppm) (cu. yds)
09-04-86
09-04-86
09-04-86
09-04-86
09-04-86
09-04-86
09-04-86
09-04-86 ND 0.02 52
09-05-86
09-05-86
09-05-86
09-05-86
09-05-86
09-05-86
09-05-86
09-05-86
09-05-86 ND 0.02 58
09-08-86
09-08-86
09-08-86
09-08-86
09-08-86
09-08-86
09-08-86
09-08-86 ND 0.02 50
09-09-86
09-09-86
09-09-86
09-09-86
09-09-86 ND 0.02 29
09-10-86
09-10-86
09-10-86
09-10-86 ND 0.02 24
09-11-86
09-11-86
09-11-86
09-11-86
09-11-86
09-11-86
09-11-86
09-11-86
09-11-86
CanonieEnvironmeritdi
-------
TABLE 1
SUMMARY OF EXCAVATION AND TREATMENT DATA
AREAS 3 AND 6
(Continued)
Area-
Caisson
Boring
Number
3-202
3-203
3-204
3-205
3-206
3-207
3-208
3-209
3-210
3-211
3-212
3-213
3-214
3-215
3-216
3-217
3-218
3-219
3-220
3-221
3-222
3-223
3-224
3-225
3-226
3-227
3-228
3-229
3-230
3-231
3-232
3-233
3-234
3-235
3-236
3-237
3-238
3-239
3-240
3-241
Locat
N129
N129
N129
N129
N135
N135
N135
N135
N130
N130
N130
N130
N130
N130
N132
N132
N132
N130
N130
N132
N130
N130
N130
N128
N128
N128
N128
N128
N131
N129
N129
N129
N129
N129
N127
N127
N127
N127
N127
N127
ion
E140
E144
E148
E152
E146
E150
E154
E158
E139
E143
E147
E151
E155
E159
E141
E145
E149
E157
E153
E143
E141
E145
E149
E139
E143
E147
E151
E155
E158
E138
E142
E146
E150
E156
E138
E142
E146
E150
E154
E134
Treated Soil
Beginning
Elevation
260
265
265
265
260
260
260
260'
260
260
260
260
260
260
260
260
260
260
260
260
260
260
260
260
265
265
265
260
260
260
260
265
265
260
270
270
265
265
265
270
Ending
Elevation
250
250
250
250
250
250
245
245
250
250
250
250
250
250
250
250
250
250
250
250
250
250
250
250
250
250
250
250
250
250
250
250
250
250
260
250
250
250
250
260
Date
Excavated
09-11-86
09-11-86
09-11-86
09-11-86
09-12-86
09-12-86
09-12-86
09-12-86
09-12-86
09-12-86
09-12-86
09-12-86
09-12-86
09-12-86
09-12-86
09-12-86
09-12-86
09-13-86
09-13-86
09-13-86
09-13-86
09-13-86
09-13-86
09-13-86
09-13-86
09-13-86
09-13-86
09-13-86
09-15-86
09-15-86
09-15-86
09-15-86
09-15-86
09-15-86
09-15-86
09-15-86
09-15-86
09-15-86
09-15-86
09-15-86
Post-
Treatment
Daily Avg.
TCE Cone.
(ppm)
Daily
Treated
Volume
(cu. yds)
ND 0.02
94
< 0.025
82
< 0.02
74
< 0.022
91
CanonieEnvironmentdi
-------
TABLE 1
SUMMARY OF EXCAVATION AND TREATMENT DATA
AREAS 3 AND 6
(Continued)
Area-
Caisson
Boring
Number
3-242
3-243
3-244
3-245
3-246
3-247
3-248
3-249
3-250
3-251
3-252
3-253
3-254
3-255
3-256
3-257
3-258
3-259
3-260
3-261
3-262
3-263
3-264
3-265
3-266
3-267
3-268
3-269
3-270
3-271
3-272
3-273
3-274
3-275
3-276
3-277
Location
N128
N128
N128
N128
N126
N126
N126
N126
N129
N126
N126
N127
N127
N127
N127
N125
N125
N125
N125
N125
N125
N125
N126
N126
N126
N126
N126
N126
N132
N125
N125
N125
N125
N125
N125
N127
E141
E145
E149
E153
E153
E149
E141
E145
E154
E133
E137
E144
E148
E152
E140
E154
E150
E146
E142
E138
E134
E130
E151
E147
E143
E139
E135
E131
E163
E152
E148
E144
E140
E136
E132
E136
Treated
Beginning
Elevation
260
265
265
265
265
265
270
270
260
270
270
265
265
265
270
265
265
270
270
270
270
270
265
265
270
270
270
270
260
265
265
270
270
270
270
270
Soil
Ending
Elevation
250
250
250
250
255
250
255
250
250
260
260
250
250
250
250
255
255
250
255
260
260
260
250
250
250
260
260
260
250
255
250
250
260
260
260
260
Post-
Treatment Daily
Daily Avg. Treated
Date TCE Cone. Volume
Excavated (ppm) (cu. yds)
09-16-86
09-16-86
09-16-86
09-16-86
09-16-86
09-16-86
09-16-86
09-16-86 ND 0.02 68
09-17-86
09-17-86
09-17-86
09-17-86
09-17-86
09-17-86
09-17-86
09-17-86
09-17-86
09-17-86
09-17-86
09-17-86
09-17-86
09-17-86 ND 0.02 106
09-18-86
09-18-86
09-18-86
09-18-86
09-18-86
09-18-86
09-18-86 ND 0.02 53
09-19-86
09-19-86
09-19-86
09-19-86
09-19-86
09-19-86
09-19-86 ND 0.02 50
CanonieEnvironmerl.
.a
-------
TABLE 1
SUMMARY OF EXCAVATION AND TREATMENT DATA
AREAS 3 AND 6
(Continued)
Area-
Caisson
Boring
Number
3-278
3-279
3-280
3-281
3-282
3-283
3-284
3-285
3-286
3-287
3-288
3-289
3-290
3-291
3-292
3-293
3-294
3-295
3-296
3-297
3-298
3-299
3-300
3-301
3-302
3-303
3-304
3-305
3-306
3-307
3-308
3-309
3-310
3-311
3-312
3-313
3-314
3-315
Location
N124
N124
N124
N124
N124
N124
N129
N122
N122
N122
N122
N122
N124
N124
N124
N124
N124
N124
N136
N136
N136
N136
N123
N123
N123
N123
N123
N123
N121
N121
N121
N122
N122
N122
N122
N136
N136
N130.5
E131
E135
E139
E143
E147
E151
E158
E153
E137
E141
E145
E149
E133
E137
E141
E145
E149
£153
E159
E155
E153
E149
E134
E138
E142
E146
E150
E154
E138
E142
E146
E139
E143
E147
E151
E151
E157
E128
Treated
Beginning
Elevation
270
270
270
270
270
265
270
265
270
270
270
270
270
270
270
270
270
265
260
260
260
260
270
270
270
270
270
270
270
270
270
270
270
270
270
260
260
265
Soil
Ending
Elevation
260
260
260
255
255
255
250
255
260
260
255
255
260
260
260
255
255
255
245
245
245
250
260
260
255
255
255
255
260
255
255
260
255
255
255
245
245
250
Date
Excavated
10-20-86
10-20-86
10-20-86
10-20-86
10-20-86
10-20-86
10-20-86
10-20-86
10-20-86
10-21-86
10-21-86
10-21-86
10-21-86
10-21-86
10-21-86
10-21-86
10-21-86
10-21-86
10-21-86
10-21-86
10-22-86
10-22-86
10-22-86
10-22-86
10-22-86
10-22-86
10-22-86
10-22-86
10-22-86
10-22-86
10-22-86
10-23-86
10-23-86
10-23-86
10-23-86
10-23-86
10-23-86
10-23-86
Post-
Treatment
Daily Avg.
TCE Cone.
(ppm)
Daily
Treated
Volume
(cu. yds)
NO 0.02
65
< 0.05
83
< 0.022
85
ND 0.02
59
CanonieEnvironme
-------
TABLE 1
SUMMARY OF EXCAVATION AND TREATMENT DATA
AREAS 3 AND 6
(Continued)
Area-
Caisson
Boring
Number
3-316
3-317
3-318
3-319
3-320
3-321
3-322
3-323
3-324
3-325
3-326
3-327
3-328
3-329
3-330
6-79
6-80
6-81
6-82
6-83
6-84
6-85
6-86
6-87
6-88
6-89
6-90
6-91
6-92
6-93
6-94
6-95
6-96
6-97
6-98
6-99
6-100
6-101
6-102
Location
N131.5
N123
N123
N123
N123
N123
N121
N121
N121
N121
N130.5
N131.5
N121
N124
N130
N115
N114
N114
N114
N114
N112
N112
N112
N112
N114
N115
N113
N113
Nlll
Nlll
Nlll
N113
N113
N113
Nlll
Nlll
Nlll
N109
N109
N109
N127
E130
E136
E140
E144
E148
E152
E140
E144
E148
E152
E130
E128
E150
E129
E137
E105
E112
E116
£108
E114
E112
E116
E120
E108
E110
E107
E119
E115
E113
E117
E121
Elll
E107
E109
E119
E115
Elll
E117
E119
E121
E118
Treated
Beginning
Elevation
260
270
270
270
270
270
270
270
270
270
260
260
265
270
260
287.5
287.5
287.5
287.5
287.5
287.5
287.5
287.5
272.5
287.5
287.5
287.5
287.5
287.5
287.5
287.5
287.5
272.5
287.5
287.5
287.5
272.5
287.5
287.5
272.5
287.5
Soil
Ending
Elevation
250
260
260
255
255
255
260
255
255
255
250
250
255
260
250
262.5
262.5
262.5
262.5
262.5
262.5
262.5
262.5
262.5
262.5
262.5
262.5
262.5
262.5
262.5
262.5
262.5
262.5
262.5
262.5
262.5
262.5
262.5
262.5
262.5
277.5
Post-
Treatment
Daily Avg.
Date TCE Cone.
Excavated (ppm)
10-24-86
10-24-86
10-24-86
10-24-86
10-24-86
10-24-86
10-24-86
10-24-86
10-24-86
10-24-86
10-24-86
10-24-86 < 0.02
10-27-86
10-27-86
10-27-86
10-27-86
10-27-86
10-27-86
10-27-86 < 0.025
10-28-86
10-28-86
10-28-86
10-28-86
10-28-86
10-28-86 ND 0.02
10-29-86
10-29-86
10-29-86
10-29-86
10-29-86
10-29-86
10-29-86
10-29-86
10-29-86 ND 0.02
10-30-86 ND 0.02
10-31-86
10-31-86
10-31-86
10-31-86
10-31-86
10-31-86
Daily
Treated
Volume
(cu. yds)
88
77
80
124
15
CanonieE
nvironmert
-------
TABLE 1
SUMMARY OF EXCAVATION AND TREATMENT DATA
AREAS 3 AND 6
(Continued)
Area-
Caisson
Boring
Number
6-103
6-104
6-105
6-106
6-107
3-331
3-332
3-333
6-108
6-109
6-110
6-111
6-112
6-113
6-114
6-115
6-116
6-117
6-118
6-119
6-120
6-121
6-122
6-123
6-124
6-125
6-126
6-127
6-128
6-129
6-130
6-131
6-132
6-133
6-134
6-135
Loc at
N126
N125
N127
N125
N125
N132.5
N133.5
N132.5
N110
N110
N110
N127
N126
N126
N126
N127
N123
N123
N123
N108
N108
N110
N110
N128
N128
N128
N128
N125
N125
N125
N125
N112
N112
N112
N108
N110
N114
N115
N116
N115
ion
E126
E118
E122
E126
E122
E127
E129
E131
E120
E116
E112
E124
E124
E122
E120
E120
E126
E122
E118
E138
E134
E138
E134
E117
E121
E125
E123
E116
E120
E124
E128
E118
E114
E110
E136
E136
E136
E133
E136
E139
Treated
Beginning
Elevation
287.5
287.5
287.5
287.5
287.5
265
265
265
287.5
287.5
272.5
287.5
287.5
287.5
287.5
287.5
287.5
287.5
287.5
287.5
287.5
287.5
287.5
287.5
287.5
287.5
287.5
287.5
287.5
287.5
287.5
287.5
287.5
272.5
287.5
287.5
277.5
277.5
277.5
277.5
Soil
Ending
Elevation
277.5
277.5
277.5
277.5
277.5
250
250
250
262.5
262.5
262.5
277.5
277.5
277.5
277.5
277.5
277.5
277.5
277.5
277.5
277.5
277.5
277.5
277.5
277.5
277.5
277.5
277.5
277.5
277. 5
277.5
262.5
262.5
262.5
277.5
277.5
267.5
267.5
267.5
267.5
Post-
Treatment Daily
Daily Avg. Treated
Date TCE Cone. Volume
Excavated (ppm) (cu. yds)
10-31-86
10-31-86
10-31-86
10-31-86
10-31-86 < 0.02 91
11-01-86
11-01-86 ND 0.02 18
11-03-86
11-03-86
11-03-86
11-03-86
11-03-86
11-03-86
11-03-86
11-03-86
11-03-86
11-03-86
11-03-86
11-03-86
11-03-86
11-03-86
11-03-86
11-03-86 < 0.02 115
11-04-86
11-04-86
11-04-86
11-04-86
11-04-86
11-04-86
11-04-86
11-04-86
11-04-86
11-04-86
11-04-86
11-04-86
11-04-86
11-04-86
11-04-86 ND 0.02 106
11-05-86
11-05-86 ND 0.02 12
CanonieEnvironn"
-------
TABLE 1
SUMMARY OF EXCAVATION AND TREATMENT DATA
AREAS 3 AND 6
(Continued)
Area-
Caisson
Boring
Number
6-136
6-137
6-138
6-139
6-140
6-141
6-142
6-143
6-144
6-145
6-146
6-147
6-148
6-149
6-150
6-151
6-152
6-153
6-154
6-155
6-156
6-157
6-158
6-159
6-160
6-161
6-162
6-163
6-164
6-165
6-166
6-167
6-168
6-169
6-170
Location
N128
N126
N126
N124
N124
N124
N124
N124
N109
N104
N104
N105
N109
N112
N114
N104
N106
N109
Nlll
N116
N116
N114
N129
N126
N123
N123
N123
N110
N110
N105
N105
N115
N117
Nlll
N110
N124
N124
N125
E119
E117
E127
E127
E123
E125
E119
E115
E115
E136
E134
E133
E135
E136
E134
E138
E134
E137
E137
E134
E138
E138
E121
E129
E124
E120
E116
E122
E114
E137
E135
E135
E135
E135
E118
E121
E117
E114
Treated
Beginning
Elevation
287.5
287.5
287.5
287.5
287.5
287.5
287.5
287.5
272-5
277.5
277.5
277.5
287.5
287.5
277.5
277.5
277.5
287.5
287.5
277.5
277.5
277.5
287.5
287.5
287.5
287.5
287.5
272.5
272.5
277.5
277.5
277.5
277.5
287.5
287.5
287.5
287.5
287.5
Soil
Ending
Elevation
277.5
277.5
277.5
277.5
277.5
277.5
277.5
277.5
262.5
267.5
267.5
267.5
277. 5
277.5
267.5
267.5
267.5
277.5
277.5
267.5
267.5
267.5
277.5
277.5
277.5
277.5
277. 5
262.5
262.5
267.5
267.5
267.5
267.5
277.5
262.5
277.5
277.5
277.5
Post-
Treatment
Daily Avg.
Date TCE Cone.
Excavated (ppm)
11-07-86
11-07-86
11-07-86
11-07-86
11-07-86
11-07-86
11-07-86
11-07-86
11-07-86
11-07-86
11-07-86
11-07-86
11-07-86
11-07-86
11-07-86 ND 0.02
11-10-86
11-10-86
11-10-86
11-10-86
11-10-86
11-10-86
11-10-86
11-10-86
11-10-86
11-10-86
11-10-86
11-10-86
11-10-86
11-10-86 ND 0.02
11-11-86
11-11-86
11-11-86
11-11-86
11-11-86
11-11-86
11-11-86
11-11-86
11-11-86 ND 0.02
Daily
Treated
Volume
(cu. yds)
94
83
62
CanonieEnvironn
lentai
-------
TABLE 1
SUMMARY OF EXCAVATION AND TREATMENT DATA
AREAS 3 AND 6
(Continued)
Area-
Caisson
Boring
Number
6-171
6-172
3-334
3-335
3-336
3-337
3-338
3-339
3-340
3-341
3-342
3-343
3-344
3-345
3-346 -
3-347
3-348
3-349
3-350
3-351
3-352
3-353
3-354
3-355
3-356
3-357
3-358
3-359
3-360
3-361
3-362
3-363
3-364
3-365
3-366
3-367
3-368
Location
N106
N115
N104
N104
N106
N106
N108
N108
N108
N108
N108
N108
N104
N106
N106
N105
N105
N107
N107
N108
N108
N108
N108
N108
N108
N105
N105
N107
N107
N110
N110
N110
N108
N108
N108
N108
N110
E136
E137
E145
E149
E145
E149
E143
E147
E151
E157
E161
E165
E147
E147
E151
E144
E148
E144
E148
E153
E159
E163
E167
E171
E175
E146
E150
E146
E150
E137
E141
E145
E145
E149
E173
E169
E139
Treated
Beginning
Elevation
277.5
277.5
275
275
275
275
275
275
270
270
270
270
275
275
275
275
275
275
275
270
270
270
270
270
270
275
275
275
275
275
270
275
275
275
270
270
275
Soil
Ending
Elevation
267.5
267.5
265
265
265
265
265
260
260
260
260
260
265
265
265
265
265
265
260
260
260
260
260
260
260
265
265
265
260
270
260
260
260
260
260
260
270
Post-
Treatment Daily
Daily Avg. Treated
Date TCE Cone. Volume
Excavated (ppm) (cu. yds)
11-12-86
11-12-86
11-12-86
11-12-86
11-12-86
11-12-86
11-12-86
11-12-86
11-12-86
11-12-86
11-12-86
11-12-86
11-12-86
11-12-86
11-12-86 ND 0.02 91
11-13-86
11-13-86
11-13-86
11-13-86
11-13-86
11-13-86
11-13-86
11-13-86
11-13-86
11-13-86
11-13-86
11-13-86
11-13-86
11-13-86
11-13-86
11-13-86
11-13-86 ND 0.02 106
11-14-86
11-14-86
11-14-86
11-14-86
11-14-86 ND 0.02 32
CanonieEnvironme:
-------
TABLE 1
SUMMARY OF EXCAVATION AND TREATMENT DATA
AREAS 3 AND 6
(Continued)
Area-
Caisson
Boring
Number
3-369
3-370
3-371
3-372
3-373
3-374
3-375
3-376
3-377
3-378
3-379
3-380
3-381
3-382
3-383
3-384
3-385
3-386
3-387
3-388
3-389
3-390
3-391
3-392
3-393
3-394
3-395
3-396
3-397
3-398
3-399
3-400
3-401
3-402
3-403
Location
N110
N110
N110
N110
N110
N110
N110
N110
N110
N110
N109
N109
N109
N110
N110
N110
N112
N112
N112
N112
N112
N112
N112
N112
N114
N118
N109
N109
N109
N109
N109
N109
N109
N109
N109
E143
E147
E151
E155
E159
E171
E167
E163
E175
E179
E142
E146
E150
E165
E169
E153
E137
E141
E145
E149
E171
E167
E163
E159
E137
E137
E144
E148
E152
E156
E160
E164
E168
E172
E176
Treated
Beginning
Elevation
275
275
270
270
270
270
270
270
275
275
270
275
275
270
270
270
275
275
275
270
270
270
270
270
275
275
275
275
270
270
270
270
270
270
275
Soil
Ending
Elevation
260
260
260
260
260
260
260
260
260
270
260
260
260
260
260
260
260
260
260
260
260
260
260
260
260
260
260
260
260
260
260
260
260
260
260
Post-
Treatment Daily
Daily Avg. Treated
Date TCE Cone. Volume
Excavated (ppm) (cu. yds)
11-18-86
11-18-86
11-18-86
11-18-86
11-18-86
11-18-86
11-18-86
11-18-86 ND 0.02 53
11-19-86
11-19-86
11-19-86 ND 0.02 18
11-20-86
11-20-86
11-20-86
11-20-86
11-20-86
11-20-86
11-20-86
11-20-86
11-20-86
11-20-86
11-20-86
11-20-86
11-20-86
11-20-86
11-20-86 < 0.02 109
11-24-86
11-24-86
11-24-86
11-24-86
11-24-86
11-24-86
11-24-86
11-24-86
11-24-86 ND 0.02 62
CanonieEnvironmc
-------
TABLE 1
SUMMARY OF EXCAVATION AND TREATMENT DATA
AREAS 3 AND 6
(Continued)
Area-
Caisson
Boring
Number
3-404
3-405
3-406
3-407
3-408
3-409
3-410
3-411
3-412
3-413
3-414
3-415
3-416
3-417
3-418
3-419
3-420
3-421
3-422
3-423
3-424
3-425
3-426
3-427
3-428
3-429
3-430
3-431
3-432
3-433
3-434
3-435
3-436
3-437
3-438
3-439
3-440
3-441
3-442
Location
N112
N109
N109
N109
N109
N109
N109
N109
N112
N112
Nlll
Nlll
Nlll
Nlll
Nlll
Nlll
N112
Nlll
Nlll
Nlll
Nlll
Nlll
Nlll
Nlll
Nlll
Nlll
N113
N113
N110
N110
N110
N110
N110
Nlll
Nlll
Nlll
Nlll
N112
N112
E139
E178
E154
E174
E170
E166
E158
E162
E143
E147
E178
E174
E170
E166
E162
E158
E151
E136
E140
E144
E148
E172
E176
E180
E152
E168
E136
E140
E157
E161
E173
E177
E181
E138
E142
E146
E150
E169
E165
Treated
Beginning
Elevation
275
275
270
275
270
270
270
270
275
275
275
275
270
270
270
270
270
275
275
275
275
275
275
275
270
270
275
275
270
270
275
275
275
275
275
275
270
270
270
Soil
Ending
Elevation
260
270
260
260
260
260
260
260
260
260
270
260
260
260
260
260
260
265
260
260
260
260
260
270
260
260
260
260
260
260
260
260
270
260
260
260
260
260
260
Post-
Treatment
Daily Avg.
Date TCE Cone.
Excavated (ppm)
11-25-86
11-25-86
11-25-86
11-25-86
11-25-86
11-25-86
11-25-86
11-25-86
11-25-86
11-25-86
11-25-86
11-25-86
11-25-86
11-25-86
11-25-86
11-25-86
11-25-86 ND 0.02
11-26-86
11-26-86
11-26-86
11-26-86
11-26-86
11-26-86
11-26-86
11-26-86
11-26-86
11-26-86
11-26-86 ND 0.02
11-28-86
11-28-86
11-28-86
11-28-86
11-28-86
11-28-86
11-28-86
11-28-86
11-28-86
11-28-86
11-28-86 ND 0.02
Daily
Treated
Volume
(cu. yds)
109
83
77
CanonieEnvironn
ie::tci;
-------
TABLE 1
SUMMARY OF EXCAVATION AND TREATMENT DATA
AREAS 3 AND 6
(Continued)
Area-
Caisson
Boring
Number
3-443
3-444
3-445
3-446
3-447
3-448
3-449
3-450
3-451
3-452
3-453
3-454
3-455
3-456
3-457
3-458
3-459
3-460
3-461
3-462
3-463
3-464
3-465
3-466
3-467
3-468
3-469
3-470
3-471
3-472
3-473
3-474
3-475
3-476
3-477
3-478
3-479
3-480
3-481
3-482
3-483
3-484
3-485
Location
N104
N103
N104
N112
N110
N103
N103
Nlll
Nlll
N112
N109
N113
N113
N114
N114
N114
N116
N116
N116
N116
N11S
N120
N102
N103
N120
N120
N120
N120
N118
N118
N118
N118
N107
N120
N120
N120
N118
N118
N102
N118
N116
N116
Nlll
E143
E148
E151
E161
E149
E146
E150
E164
E160
E178
E140
E138
E142
E139
E143
E147
E147
E151
E139
E143
E139
E139
E147
E144
E141
E149
E153
E145
E141
E153
E149
E145
E153
E143
E147
E151
E143
E151
E145
E147
E141
E145
E134
Treated
Beginning
Elevation
275
275
275
270
275
275
275
270
270
275
275
275
275
275
275
265
265
265
275
270
275
270
275
275
270
265
265
270
270
265
265
270
275
270
265
265
270
265
275
265
275
270
275
Soil
Ending
Elevation
265
265
265
260
260
265
265
260
260
270
260
260
260
260
255
255
255
255
255
255
255
260
265
265
255
255
255
255
255
255
255
255
260
255
255
255
255
255
265
255
255
255
265
Post-
Treatment Daily
Daily Avg. Treated
Date TCE Cone. Volume
Excavated (ppm) (cu. yds)
12-01-86
12-01-86
12-01-86
12-01-86
12-01-86 ND 0.02 32
12-02-86
12-02-86
12-02-86
12-02-86
12-02-86
12-02-86
12-02-86
12-02-86 ND 0.02 53
12-04-86
12-04-86
12-04-86
12-04-86
12-04-86
12-04-86
12-04-86
12-04-86
12-04-86 < 0.02 77
12-05-86
12-05-86
12-05-86
12-05-86
12-05-86
12-05-86
12-05-86
12-05-86
12-05-86
12-05-86
12-05-86 < 0.032 80
12-08-86
12-08-86
12-08-86
12-08-86
12-08-86
12-08-86
12-08-86
12-08-86
12-08-86
12-08-86 ND 0.02 74
CanonieEnvironrr
-------
TABLE 1
SUMMARY OF EXCAVATION AND TREATMENT DATA
AREAS 3 AND 6
(Continued)
Area-
Caisson
Boring
Number
3-486
3-487
3-488
3-489
3-490
3-491
3-492
3-493
3-494
3-495
3-496
3-497
3-498
3-499
3-500
3-501
3-502
3-503
3-504
3-505
3-506
3-507
3-508
3-509
3-510
3-511
3-512
3-513
3-514
3-515
3-516
3-517
3-518
Location
N102
N110
N119
N119
N119
N119
N117
N117
N117
N117
N103
N115
N115
N115
N115
N117
N117
N117
N117
N114
N114
N114
N116
N119
N119
N119
N119
N120
N113
N113
N115
N115
N115
E143
E135
E138
E142
E146
E150
E138
E142
E146
E150
E142
E146
E142
E138
E150
E144
E148
E152
E140
E141
E145
E149
E149
E152
E148
E144
E140
E137
E144
E146
E140
E144
E148
Treated
Beginning
Elevation
275
275
270
270
265
265
275
270
265-
265
275
265
275
275
265
270
265
265
275
275
275
265
265
265
265
270
270
270
275
275
275
270
265
Soil
Ending
Elevation
265
270
260
255
255
255
255
255
255
255
265
255
255
260
255
255
255
255
255
260
255
255
255
255
255
255
255
260
260
260
255
255
255
Post-
Treatment
Daily Avg.
Date TCE Cone.
Excavated (ppm)
12-09-86
12-09-86
12-09-86
12-09-86
12-09-86
12-09-86
12-09-86
12-09-86
12-09-86
12-09-86 NO 0.02
12-10-86
12-10-86
12-10-86
12-10-86
12-10-86
12-10-86
12-10-86
12-10-86
12-10-86 ND 0.02
12-11-86
12-11-86
12-11-86
12-11-86
12-11-86
12-11-86
12-11-86
12-11-86
12-11-86
12-11-86 ND 0.02
12-12-86
12-12-86
12-12-86
12-12-86 ND 0.02
Daily
Treated
Volume
(cu. yds)
68
71
77
35
CanonieEnvironmenta I
-------
TABLE 2
SUMMARY OF EXCAVATION AND TREATMENT DATA
AREAS Kb), 4, and 8
TCE Concentration (ppm) Daily Treated
Location
Area 4
Area 4
Areas 3 and 4
Areas 3 and 4
Area 4
Area 3
Area 4
Area 4
Area IB
Area IB
Area IB
Area IB
Area IB
Area IB
Area 8
Area 8
Area 8
Area 8
Area 8
Date Excavated
12-12-86
12-15-86
12-16-86
12-17-86
12-18-86
12-19-86
12-29-86
12-30-86
12-31-86
01-02-87
01-05-87
01-06-87
01-07-87
01-08-87
01-09-87
01-12-87
01-13-87
01-14-87
01-15-87
Post-Treatment Daily Ave.
ND 0.02
<0.028
<0.08
<0.07
<0.063
<0.054
ND 0.02
ND 0.02
ND 0.02
<0.081
ND 0.02
ND 0.02
<0.047
ND 0.02
<0.44
<0.061
NO 0.02
ND 0.02
ND 0.02
Volume (c.y.)
26
98
107
56
100
76
74
104
110
63
84
105
133
110
126
102
112
63
116
Rerun Material
from 01-09-87
Rerun Material
01-16-87
ND 0.02
77
from 01-09-87
Area 8
Area 8
Area 8
Area 8
Area 8
Area 8
Area 8
Area 8
Area 8
Area 8
Areas 4, 6, and 8
01-19-87
01-20-87
01-21-87
01-22-87
01-23-87
01-26-87
01-27-87
01-28-87
01-29-87
01-30-87
02-02-87
02-03-87
ND 0.02
<0.022
NO 0.02
<0.02
<0.02
ND 0.02
<0.024
<0.021
NO 0.02
<0.02
<0.02
ND 0.02
72
102
56
84
70
77
91
94
10
70
77
101
CanonieEnvironmentdi
-------
TABLE 3
SUMMARY OF TCE CONCENTRATIONS
EXCAVATION PERIMETER SAMPLES
AREA 1-8
Sample
Sample Depth Elevation TCE Concentration
Sample No.
1-8-18-1
1-8-1B-2
1-8-1B-3
1-8-1B-4
1-8-1B-5
1-8-1B-6
1-8-1B-7
1-9-1B-8
1-9-1B-9
1-9-1B-10
1-9-1B-11
1-9-1B-12
1-9-1B-13
1.9-18-14
(ft.)
8.0
8.0
8.0
8.0
8.0
8.0
8.0
8.0
16.0
16.0
16.0
16.0
16.0
16.0
(Ft)
290.0
290.0
290.0
290.0
290.0
290.0
290.0
290.0
282.0
282.0
282.0
282.0
282.0
282.0
Perimeter
Lateral
Lateral
Lateral
Lateral
Lateral
Lateral
Lateral
Lateral
Vertical
Vertical
Vertical
Vertical
Vertical
Vertical
(ppm)
ND 0.02
ND 0.02
ND 0.02
ND 0.02
ND 0.02
ND 0.02
ND 0.02
ND 0.02
ND 0.02
ND 0.02
ND 0.02
ND 0.02
ND 0.02
ND 0.02
CanonieEnvlronmentdl
-------
TABLE 3
SUMMARY OF TCE CONCENTRATIONS
EXCAVATION PERIMETER SAMPLES
AREA 3
(Continued)
Hole No.
9-4-159
9-5-171
9-8-181
9-9-184
9-10-189
9-10-19U
9-11-196
9-12-206
9-12-215
9-12-216
9-13-225
9-13-229
9-15-231
9-15-240
9-15-241
9-16-246
9-17-257
9-17-263
9-18-269
9-18-270
10-20-284
10-20-285
10-21-295
10-21-296
10-21-297
10-22-298
10-22-299
Location
N 134
N 134
N 131
N 133
N 133
N 131
N 135
N 135
N 130
N 132
N 128
N 128
N 129
N 127
N 127
N 126
N 125
N 125
N 126
N 132
N 129
N 122
N 124
N 136
N 136
N 136
N 136
E 161
E 143
E 162
N 162
E 142
E 140
E 160
E 146
E 159
E 141
E 139
E 155
E 138
E 154
E 134
E 153
E 154
E 130
E 131
E 163
E 158
E 153
E 153
E 159
E 155
E 153
E 149
TCE Concentration
(ppm)
ND 0.02
ND 0.02
ND 0.02
ND 0.02
ND 0.02
ND 0.02
ND 0.02
ND 0.02
0.48
ND 0.02
0.13
ND 0.02
0.27
ND 0.02
0.04
0.04
0.08
0.82
ND 0.02
ND 0.02
0.03
0.11
0.06
ND 0.02
ND 0.02
ND 0.02
0.02
Sample
Elevation
256.0
255.0
255.0
255.0
255.0
254.0
255.0
255.0
255.0
255.0
255.0
255.0
254.0
258.0
265.0
260.0
260.0
264.0
265.0
255.0
255.0
260.0
260.0
250.0
250.0
253.0
255.0
CanonieEnvironmentai
-------
TABLE 3
SUMMARY OF TCE CONCENTRATIONS
EXCAVATION PERIMETER SAMPLES
AREA 3
(Continued)
Hole No.
10-22-305
10-23-313
10-23-314
10-27-325E
10-27-326E
10-27-326S
10-27-327W
10-27-329
10-27-330
11-1-331W
11-3-333E
11-12-336
11-12-338
11-12-341
11-12-342
11-12-343
11-12-346
11-13-349
11-13-352
11-13-353
11-13-354
11-13-355
11-13-356
11-13-358
11-13-360
11-13-361
11-14-366
Location
N 123
N 136
N 136
N 121
N 131 •
N 130
N 131
N 124
N 130
N 132.5
N 132.5
N 106
N 108
N 108
N 108
N 108
N 106
N 107
N 108
N 108
N 108
N 108
N 108
N 105
N 107
N 110
N 108
E 154
E 151
E 157
E 154
E 132
E 129
E 126
E 129
E 137
E 125
E 133
E 145
E 143
E 157
E 161
E 165
E 151
E 144
E 159
E 163
E 167
E 171
E 175
E 150
E 150
E 137
E 173
TCE Concentration
(ppm)
NO 0.02
NO 0.02
NO 0.02
0.08
0.02
ND 0.02
0.22
ND 0.02
NO 0.02
ND 0.02
0.04
0.4
ND 0.20
ND 0.20
ND 0.20
ND 0.20
ND 0.02
ND 0.02
ND 0.02
ND 0.02
ND 0.02
ND 0.02
ND 0.02
ND 0.02
ND 0.02
0.03
ND 0.02
Sample
Elevation
262.0
253.0
253.0
260.0
255.0
255.0
255.0
265.0
255.0
255.0
255.0
269.0
269.0
265.0
265.0
265.0
270.0
270.0
264.0
265.0
265.0
265.0
265.0
270.0
268.0
271.0
265.0
CanonieEnvironmentdi
-------
TABLE 3
SUMMARY OF TCE CONCENTRATIONS
EXCAVATION PERIMETER SAMPLES
AREA 3
(Continued)
Hole No.
11-14-367
11-14-368
11-20-389
11-20-390
11-20-391
11-20-392
11-25-405
11-25-415
11-25-419
11-25-420
11-26-426
11-26-427
11-26-428
11-28-436
11-28-441
11-28-442
12-1-145W
12-1-153W
12-1-148W
12-1-39W
12-1-14W
12-1-56W
12-1-62W
12-1-72W
12-1-89W
12-1-101W
12-1-110W
Location
N 108
N 110
N 112
N 112
N 112
N 112
N 109
N 111
N 111
N 112
N 111
N 111
N 111
N 110
N 112
N 112
N 108
N 109
N 110
N 111
N 115
N 116
N 117
N 118
N 119
N 120
N 121
E 169
E 139
E 171
E 167
E 163
E 159
E 178
E 174
E 158
E 151
E 176
E 180
E 152
E 181
E 169
E 165
E 115
E 114
E 115
E 114
E 114
E 113
E 114
E 115
E 114
E 115
E 116
TCE Concentration
(ppm)
NO 0.02
NO 0.02
ND 0.02
NO 0.02
NO 0.02
ND 0.02
0.04
ND 0.02
ND 0.02
0.06
ND 0.02
ND 0.02
ND 0.02
0.35
ND 0.02
ND 0.02
0.03
ND 0.02
ND 0.02
0.70
ND 0.02
ND 0.02
ND 0.02
ND 0.02
ND 0.02
ND 0.02
ND 0.02
Sample
Elevation
265.0
272.0
265.0
265.0
265.0
265.0
272.0
265.0
265.0
265.0
265.0
272.0
265.0
272.0
265.0
265.0
285.0
285.0
285.0
285.0
270.0
285.0
285.0
285.0
285.0
285.0
285.0
CanonieEnvironmentdl
-------
TABLE 3
SUMMARY OF TCE CONCENTRATIONS
EXCAVATION PERIMETER SAMPLES
AREA 3
(Continued)
Hole No.
12-1-120W
12-1-129NW
12-1-135N
12-1-443
12-1-445
12-1-446
12-2-449
12-2-452
12-2-453
12-4-460
12-5-465
12-5-469
12-5-472
12-5-475
12-8-481
12-9-486
12-9-487
12-10-496
12-10-500
12-10-503
12-11-507
12-11-509
12-11-NllO E132
12-11-388 NW
12-11-372N
12-11-351E
12-12-347W
Location
N 122
N 124
N 124
N 104
N 104
N 112
N 103
N 112
N 109
N 116
N 102
N 120
N 118
N 107
N 102
N 102
N 110
N 103
N 115
N 117
N 114
N 119
N 110
N 113
N 111
N 108
N 105
E 117
E 121
E 126
E 143
E 151
E 161
E 150
E 178
E 140
E 151
E 147
E 153
E 153
E 153
E 145
E 143
E 135
E 142
E 150
E 152
E 149
E 152
E 132
E 148
E 155
E 155
E 142
TCE Concentration
(ppm)
ND 0.02
0.12
ND 0.02
0.24
ND 0.02
ND 0.02
ND 0.02
ND 0.02
ND 0.02
ND 0.02
0.06
ND 0.02
ND 0.02
ND 0.02
ND 0.02
ND 0.02
ND 0.02
ND 0.02
ND 0.02
0.04
0.02
NO 0.02
ND 0.02
ND 0.02
ND 0.02
ND 0.02
0.08
Sample
Elevation
285.0
285.0
285.0
269.0
270.0
265.0
270.0
272.0
265.0
260.0
270.0
260.0
260.0
265.0
270.0
270.0
272.0
270.0
260.0
260.0
260.0
260.0
270.0
265.0
267.0
265.0
270.0
CanonieEnvironmentd
-------
Hole No.
12-16-N129 E108
12-16-N127 E105
12-16-N127 Elll
12-16-N125 E108
12-17-N115 E112
12-17-N114 E110
12-17-N113 Elll
12-17-N112 Elll
12-17-N111 E113
12-17-N125 E125
12-17-N125 E123
12-19-N107 E118
12-19-N107 E122
12-19-N106 E115
12-19-N105 E125
12-19-N104 E117
12-19-N103 E122
12-19-N108 E127
12-19-N109 E128
12-19-N110 E130
1-19-N123 E119
1-20-N134 E127
1-20-N134 E131
1-20-N128 E136
1-20-N135.5 E129
TABLE 3
SUMMARY OF TCE CONCENTRATIONS
EXCAVATION PERIMETER SAMPLES
AREA 3
(Continued)
Location
N 129
N 127
N 127
N 125
N 115
N 114
N 113
N 112
N 111
N 125
N 125
N 107
N 107
N 106
N 105
N 104
N 103
N 108
N 109
N 110
N 123
N 134
N 134
N 128
N 135.5
E 108
E 105
E 111
E 108
E 112
E 110
E 111
E 111
E 113
E 125
E 123
E 118
E 122
E 115
E 125
E 117
E 122
E 127
E 128
E 130
E 119
E 127
E 131
E 136
E 129
TCE Concentration
(ppm)
ND 0.02
0.03
0.03
0.04
0.06
0.05
0.03
0.04
ND 0.02
ND 0.02
0.06
ND 0.02
ND 0.02
ND 0.02
ND 0.02
ND 0.02
ND 0.02
ND 0.02
ND 0.02
ND 0.02
ND 0.02
0.02
0.02
0.64
ND 0.02
Sample
Elevation
265.0
265.0
265.0
265.0
282.0
282.0
282.0
282.0
282.0
280.0
280.0
280.0
280.0
280.0
280.0
280.0
280.0
285.0
285.0
285.0
285.0
255.0
255.0
265.0
255.0
CanonieEnvironmenta;
-------
TABLE 3
SUMMARY OF TCE CONCENTRATIONS
EXCAVATION PERIMETER SAMPLES
AREA 4
(Continued)
Sample No.
12-15-A4-1
12-15-A4-2
12-15-A4-4
12-15-A4-5
12-18-A4-6
12-18-A4-7
12-18-A4-8
12-18-A4-9
12-18-A4-10
12-30-A4-11
12-30-A4-12
12-30-A4-13
12-30-A4-14
12-30-A4-15
12-30-A4-16
12-30-A4-17
2-3-A4-18
2-3-A4-19
2-3-A4-20
Sample Depth
(ft.)
10.5
5.5
5.5
5.5
5.5
5.5
11.0
11.0
10.5
11.0
16.0
16.0
8.0
8.0
8.0
8.0
10.5
10.5
5.5
Sample
Elevation
(Ft)
280.5
285.5
285.5
285.5
285.5
285.5
280.0
280.0
280.5
280.0
275.0
275.0
283.0
283.0
283.0
283.0
280.5
280.5
285.5
Perimeter
Vertical
Lateral
Lateral
Lateral
Lateral
Lateral
Vertical
Vertical
Vertical
Vertical
Vertical
Vertical
Lateral
Lateral
Lateral
Lateral
Vertical
Vertical
Lateral
TCE Concentration
(ppm)
ND 0.02
NO 0.02
ND 0.02
0.02
0.09
0.10
0.11
0.11
0.14
ND 0.02
ND 0.02
ND 0.02
ND 0.02
ND 0.02
ND 0.02
ND 0.02
0.17
0.17
ND 0.02
CanomeEnvironmenta
-------
TABLE 3
SUMMARY OF TCE CONCENTRATIONS
EXCAVATION PERIMETER SAMPLES
AREA 6
(Continued)
Hole No.
8-21-20
8-21-22
8-21-24
8-22-30
8-25-45
8-27-52
9-2-68
9-3-75
9-22-67W
9-22-45S
9-22-39NW
9-22-8W
9-22-17N
9-22-2W
9-22-6N
9-22-6E
9-22-9E
9-22-3E
9-22-HNE
9-22-58E
10-27-79
10-28-86
10-28-87
10-29-94
10-29-96
10-31-99
10-31-100
Location
N 121
N 119
N 119
N 117
N 117
N 116
N 115
N 113
N 114
N 116
N 119
N 120.5
N 121
N 122
N 123
N 122
N 121
N 120
N 118.5
N 114
N 115
N 112
N 112
N 111
N 113
N 111
N 109
E 117
E 127
E 109
E 127
E 105
E 124
E 123
E 121
E 104
E 104
E 105
E 110
E 114
E 118
E 126
E 128
E 129
E 130
E 130
E 124
E 105
E 120
E 108
E 121
E 107
E 111
E 117
TCE Concentration
(ppm)
0.05
0.04
ND 0.02
0.05
ND 0.02
ND 0.02
0.04
0.05
ND 0.02
ND 0.02
ND 0.02
ND 0.02
0.04
0.04
0.17
0.06
ND 0.02
0.02
ND 0.02
ND 0.02
ND 0.02
0.03
ND 0.02
ND 0.02
ND 0.02
ND 0.02
ND 0.02
Sample
Elevation
282.5
275.5
272.5
283.5
279.5
283.5
270.5
270.5
279.5
279.5
279.5
279.5
279.5
282.5
283.5
283.5
283.5
283.5
283.5
279.5
282.5
280.5
267.5
280.5
267.5
267.5
267.5
CanonieEnvironmerlai
-------
TABLE 3
SUMMARY OF TCE CONCENTRATIONS
EXCAVATION PERIMETER SAMPLES
AREA 6
(Continued)
Hole No.
10-31-101
10-31-102
11-3-116
11-3-117
11-3-118
11-3-119
11-4-130
11-4-132
11-5-135
11-5-N123
11-5-N124
11-5-N125
11-5-N126
11-5-N129
11-5-N129
11-5-N129
11-5-N128
11-5-N127
11-5-N125
11-5-N124
11-7-143
11-7-144
11-7-145
11-7-146
11-7-147
11-7-148
11-10-149
Location
E115
E113
E113
E115
E119
E123
E125
E127
E128
E130
E130
N
N
N
N
N
N
N
N
N
N
N
N
N
N
N
N
N
N
N
N
N
N
N
N
N
N
N
109
127
108
108
110
110
108
114
115
123
124
125
126
129
129
129
128
127
125
124
109
104
105
109
112
114
104
E
E
E
E
E
E
E
E
E
E
E
E
E
E
E
E
E
E
E
E
E
E
E
E
E
E
E
121
118
138
134
138
134
136
136
139
115
113
113
115
119
123
125
127
128
130
130
115
136
133
135
136
134
138
TCE Concentration
(ppm)
NO
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
.02
.28
.02
.02
.02
.04
.02
.02
.02
.04
.58
.02
.02
.03
.86
.05
.10
.11
.11
.02
.04
.02
.02
.02
.02
.02
.02
Sample
Elevation
267.
282.
280.
280.
280.
280.
280.
270.
270.
282.
282.
282.
282.
282.
282.
282.
282.
282.
282.
282.
267.
270.
270.
280.
280.
5
5
0
0
0
0
0
0
0
5
5
5
5
5
5
5
5
5
5
5
5
0
0
0
0
270.0
270.0
CanonieEnvironmentdi
-------
TABLE 3
SUMMARY OF TCE CONCENTRATIONS
EXCAVATION PERIMETER SAMPLES
AREA 6
(Continued)
Hole No.
11-10-150
11-10-151
11-10-152
11-10-153
11-10-154
11-10-155
11-10-156N
11-10-157E
11-10-133W
11-10-161
11-11-163
11-11-165
11-11-166
11-11-170
11-12-171
1-20-N110 E110
2-5-N128 E 116
Location
N 106
N 109
N 111
N 116
N 116
N 114
N 130
N 126
N 115
N 110
N 105
N 117
N 111
N 125
N 106
N 110
N 128
E 134
E 137
E 137
E 134
E 138
E 138
E 121
E 131
E 131
E 122
E 137
E 135
E 135
E 114
E 136
E 110
E 116
TCE Concentration
(ppm)
ND 0.02
ND 0.02
ND 0.02
ND 0.02
ND 0.02
ND 0.02
0.16
0.15
0.04
0.08
ND 0.02
0.02
ND 0.02
0.02
ND 0.02
ND 0.02
ND 0.02
Sample
Elevation
270.0
280.0
280.0
270.0
270.0
270.0
282.5
282.5
270.0
265.0
270.0
270.0
280.0
277.5
270.0
265.0
282.5
CanonieEnvironmentdl
-------
TABLE 3
SUMMARY OF TCE CONCENTRATIONS
EXCAVATION PERIMETER SAMPLES
AREA 8
(Continued)
Sample Depth
Sample No. (ft.)
1-22-A8-1
1-22-A8-2
1-22-A8-3
1-22-A8-4
1-22-A8-5
1-27-A8-6
1-27-A8-7
1-27-A8-8
1-27-A8-9
1-27-A8-10
1-29-A8-11
1-29-A8-12
1-30-A8-13
1-30-A8-14
1-30-A8-15
2-2-A8-16
2-2-A8-17
2-2-A8-18
2-2-A8-19
2-2-A8-20
2-3-A8-21
2-3-A8-22
2-3-A8-23
2-3-A8-24
8.0
15.0
15.0
8.0
8.0
8.0
8.0
8.0
17.0
8.0
8.0
8.0
18.0
21.0
8.0
21.0
21.0
18.0
18.0
9.0
5.0
5.0
5.0
10.0
Sample
Elevation
(Ft)
282.0
275.0
275.0
282.0
282.0
282.0
282.0
282.0
273.0
282.0
282.0
282.0
272.0
269.0
282.0
269.0
269.0
272.0
272.0
281.0
285.0
285.0
285.0
280.0
Perimeter
Lateral
Vertical
Vertical
Lateral
Lateral
Lateral
Lateral
Lateral
Vertical
Lateral
Lateral
Lateral
Vertical
Vertical
Lateral
Vertical
Vertical
Vertical
Vertical
Lateral
Lateral
Lateral
Lateral
Vertical
TCE Concentration
(ppm)
NO 0.02
ND 0.02
0.04
0.14
ND 0.02
0.05
0.02
0.02
0.03
ND 0.02
0.02
ND 0.02
0.04
0.04
ND 0.02
ND 0.02
0.02
0.03
0.05
0.28
0.02
0.02
0.02
ND 0.02
CanonieEnvironmentcii
-------
TABLE 4
AREAS IB,3,4,4,AND 8 EICAVATION VERIFICATION ANALVBIS
Rttulti in
Sup)* I.D.
8-21 20 At
8-21 22 At
8-21 24 At
8-22 30 At
8-23 43 At
8-27 32 At
9-2 AI At
9-3 73 At
9-4 139 A3
9-3 171 A3
9-8 181 A3
9-9 184 A3
9-10 189 A3
9-10 190 A3
9-11 194 A3
9-12 204 A3
9-12 213 A3
9-12 214 A3
9-13 223 A3
9-13 229 A3
9-15 231 A3
9-15 240 A3
9-13 241 A3
9-16 24t A3
9-17 237 A3
9-17 243 A3
9-18 249 A3
9-18 270 A3
9-22 2* At
9-22 17N At
9-22 BH At
9-22 39NN A*
9-22 438 At
9-22 t7N At
9-22 IIME At
9-22 3E At
9-22 9E At
9-22 4E At
9-22 tN At
9-22 38E At
10-20 284 A3
10-20 283 A3
10-21 293 A3
10-21 294 A3
10-21 297 A3
10-22 298 A3
10-22 299 A3
10-22 303 A3
L«b I.D.
A9I3
A917
A923
A92B
A93t
A944
A 1000
AIOIO
A1024
A1043
AI042
A 1048
A1073
A1072
A1083
A 1094
A2009
A2008
A2024
A2023
A2039
A2043
A2043
A2034
A2043
A2072
A2081
A2080
A2097
A209t
A2093
A2094
A2093
A2092
A2103
A2I04
A2I03
A2102
A2101
A2I04
A2I20
A2II9
A2133
A2I39
A2138
A2I42
A2143
A2134
1,2-OCB
NO 0.02
0.09
MB 0.02
0.18
NB 0.02
NO 0.02
NB 0.02
NB 0.02
NB 0.02
NB 0.02
NB 0.02
NB 0.02
NB 0.02
NB 0.02
NO 0.02
NO 0.02
NO 0.02
NB 0.02
NO 0.02
NO 0.02
0.07
NO 0.02
NO 0.04
NO 0.04
NO 0.02
NO 0.04
NO 0.02
NO 0.02
NB 0.02
NO 0.02
NO 0.02
NO 0.02
NO 0.02
NO 0.02
NO 0.02
NO 0.02
NB 0.02
NB 0.02
0.34
NO 0.02
NO 0.02
NO 0.02
NO 0.02
NO 0.02
NO 0.02
NO 0.02
NO 0.02
NO 0.02
TRANS 1,1,1-
1,3-OCB 1,4-DCO 1,2-DCE PCE TCA
NO 0.02 NO 0.02 NO 0.02 ND 0.02 ND 0.02
NO 0.02 ND 0.02 ND 0.02 ND 0.02 ND 0.02
NO 0.02 ND 0.02 ND 0.02 ND 0.02 ND 0.02
ND 0.02 ND 0.02 ND 0.02 ND 0.02 ND 0.02
NB 0.02 ND 0.02 NO 0.02 NO 0.02 NO 0.02
NO 0.02 NO 0.02 NO 0.02 NO 0.02 NO 0.02
NO 0.02 ND 0.02 NO 0.02 NO 0.02 ND 0.02
ND 0.02 NO 0.02 ND 0.02 ND 0.02 NO 0.02
NO 0.02 ND 0.02 ND 0.02 ND 0.02 ND 0.02
NO 0.02 ND 0.02 NO 0.02 ND 0.02 ND 0.02
NB 0.02 ND 0.02 ND 0.02 ND 0.02 NO 0.02
ND 0.02 ND 0.02 ND 0.02 NO 0.02 ND 0.02
NO 0.02 NO 0.02 ND 0.02 ND 0.02 ND 0.02
ND 0.02 NO 0.02 ND 0.02 ND 0.02 ND 0.02
NO 0.02 NO 0.02 NO 0.02 NO 0.02 NO 0.02
NO 0.02 NO 0.02 ND 0.02 ND 0.02 ND 0.02
ND 0.02 ND 0.02 NO 0.02 ND 0.02 ND 0.02
ND 0.02 ND 0.02 ND 0.02 ND 0.02 ND 0.02
NO 0.02 ND 0.02 NO 0.02 ND 0.02 NO 0.02
NO 0.02 NO 0.02 NO 0.02 ND 0.02 NO 0.02
ND 0.02 NO 0.02 NO 0.02 ND 0.02 ND 0.02
ND 0.02 ND 0.02 ND 0.02 ND 0.02 0.02
NO 0.04 NO 0.04 ND 0.04 ND 0.04 NO 0.04
ND 0.04 ND 0.04 NO 0.04 ND 0.04 NO 0.04
ND 0.02 NO 0.02 ND 0.02 ND 0.02 ND 0.02
NO 0.04 NO 0.04 NO 0.04 NO 0.04 NO 0.04
ND 0.02 NO 0.02 NO 0.02 NO 0.02 NO 0.02
ND 0.02 ND 0.02 ND 0.02 HD 0.02 ND 0.02
NO 0.02 NO 0.02 ND 0.02 NO 0.02 NO 0.02
NO 0.02 ND 0.02 ND 0.02 ND 0.02 NO 0.02
NO 0.02 NO 0.02 NO 0.02 ND 0.02 NO 0.02
NO 0.02 ND 0.02 ND 0.02 ND 0.02 ND 0.02
HO 0.02 ND 0.02 ND 0.02 ND 0.02 NO 0.02
NO 0.02 NO 0.02 ND 0.02 NO 0.02 ND 0.02
ND 0.02 ND 0.02 ND 0.02 ND 0.02 ND 0.02
NO 0.02 ND 0.02 NO 0.02 NO 0.02 ND 0.02
ND 0.02 ND 0.02 ND 0.02 NO 0.02 ND 0.02
ND 0.02 NO 0.02 ND 0.02 ND 0.02 NO 0.02
NO 0.02 NO 0.02 NO 0.02 ND 0.02 ND 0.02
ND 0.02 NO 0.02 ND 0.02 0.04 ND 0.02
ND 0.02 ND 0.02 ND 0.02 ND 0.02 NO 0.02
NO 0.02 NO 0.02 NO 0.02 ND 0.02 ND 0.02
NO 0.02 NO 0.02 ND 0.02 NO 0.02 ND 0.02
NO 0.02 ND 0.02 ND 0.02 ND 0.02 ND 0.02
NO 0.02 ND 0.02 ND 0.02 NO 0.02 ND 0.02
ND 0.02 ND 0.02 ND 0.02 ND 0.02 ND 0.02
NO 0.02 HD 0.02 NO 0.02 HD 0.02 ND 0.02
ND 0.02 NO 0.02 NO 0.02 ND 0.02 NO 0.02
TCE
0.03
0.04
NO 0.02
0.03
ND 0.02
ND 0.02
0.04
0.03
ND 0.02
ND 0.02
ND 0.02
ND 0.02
ND 0.02
ND 0.02
NO 0.02
ND 0.02
0.48
ND 0.02
0.13
ND 0.02
0.27
ND 0.02
ND 0.04
NO 0.04
0.08
0.82
ND 0.02
ND 0.02
0.04
0.04
ND 0.02
ND 0.02
ND 0.02
NO 0.02
0.02
NO 0.02
0.02
o.ot
0.17
ND 0.02
0.03
0.11
o.ot
NO 0.02
ND 0.02
NO 0.02
0.02
ND 0.02
Bintint
ND
ND
NO
HO
ND
NO
NO
ND
NO
ND
ND
ND
ND
NO
HO
NO
NO
ND
ND
ND
ND
NO
ND
HO
HO
HO
HD
ND
NO
ND
NO
ND
ND
ND
ND
HO
HD
ND
NO
HD
HD
HD
HD
HD
HO
HD
NO
ND
.0
.0
.0
.0
.0
.0
.0
.0
.0
.0
.0
.0
.0
.0
.0
.0
.0
.0
.0
.0
.0
.0
.0
.0
.0
.0
.0
.0
.0
.0
.0
.0
.0
.0
.0
.0
.0
.0
.0
.0
.0
.0
.0
.0
.0
.0
.0
.0
Ethyl
Bcntini
HO
ND
ND
HD
HD
HO
HD
HO
HD
NO
ND
ND
ND
HD
HO
HO
HO
HD
NO
ND
NO
ND
NO
NO
ND
NO
NO
NO
ND
NO
NO
ND
NO
NO
NO
ND
NO
NO
NB
NB
NB
ND
NO
HD
HD
ND
HD
HO
.0
.0
.0
.0
.0
.0
.0
.0
.0
.0
.0
.0
.0
.0
.0
.0
.0
.0
.0
.0
.0
.0
.0
.0
.0
.0
.0
.0
.0
.0
.0
.0
.0
.0
.0
.0
.0
.0
.0
.0
.0
.0
.0
.0
.0
.0
.0
.0
Tolutni
ND
NO
NO
NO
ND
ND
ND
ND
ND
NO
NO
NO
NO
ND
NO
ND
HO
HD
NO
ND
ND
HO
HD
HO
HD
ND
HD
HO
NO
HD
HD
HD
HO
HD
HD
ND
NO
NO
HO
HD
HO
HD
ND
ND
ND
ND
NO
.0
.0
.0
.0
.0
.0
.0
.0
.0
.0
.0
.0
.0
.0
.0
.0
.0
.0
.0
.0
.0
.0
.0
.0
.0
.0
.0
.0
.0
.0
.0
.0
.0
.0
.0
.0
.0
.0
.0
.0
.0
.0
.0
.0
.0
.0
.0
HD .0
Xylenii
NO 1.0
ND
ND
ND
NO
ND
NO
ND
HD
NO
HD
HO
HD
HD
HO
HD
1.0
HD
HD
HD
ND
ND
ND
HD
HO
HD
ND
HO
HD
HD
HD
HD
HO
NO
NO
HD
HO
HD
HD
HO
HD
HO
HO
ND
HD
NO
NO
.0
.0
.0
.0
.0
.0
.0
.0
.0
.0
.0
.0
.0
.0
.0
.0
.0
.0
.0
.0
.0
.0
.0
.0
.0
.0
.0
.0
.0
.0
.0
.0
.0
.0
.0
.0
.0
.0
.0
.0
.0
.0
.0
.0
.0
NO .0
CanomeEnvircnmental
Notti ND I dinotn noni dtttcttd to » Itvtl o< I.
-------
TABLE 4
AREAS IB,3,4,6,AND B EfcCAVATION VERIFICATION ANALYSIS
Rtiultt in
(Continued)
TRANS 1,1.1- Ethyl
Sicpl* I.D. Lab 1.0. 1,2-DCI 1,3-BCB 1,4-DCB 1,2-DCE PCE TCA TCE Binitn* Binunt Tolutn* lyltntt
10-23 31) A3 A21t3 ND 0.02 NB 0.02 NO 0.02 ND 0.02 NO 0.02 ND 0.02 NB 0.02 NB
10-23 314 A3 A2164 NB 0.02 NO 0.02 NO 0.02 ND 0.02 ND 0.02 ND 0.02 NO 0.02 ND
10-27 71 At A2I99 NB 0.02 NB 0.02 NO 0.02 NO 0.02 ND 0.02 ND 0.02 ND 0.02 ND
10-27 323E A3 A219I NB 0.02 NB 0.02 ND 0.02 ND 0.02 ND 0.02 ND 0.02 O.OB NO
10-27 32tE A3 A2190 NB 0.02 NB 0.02 NB 0.02 ND 0.02 NB 0.02 NB 0.02 0.02 NB
10-27 32tB A3 A2I92 NB 0.02 NB 0.02 NB 0.02 NO 0.02 ND 0.02 ND 0.02 ND 0.02 ND
10-27 327N A3 A2I09 NB 0.02 NB 0.02 NB 0.02 ND 0.02 NB 0.02 ND 0.02 0.22 ND
10-27 329 A3 A21B3 NB 0.02 NB 0.02 NO 0.02 ND 0.02 ND 0.02 NO 0.02 0.02 NB
10-27 330 A3 A2IB9 NB 0.02 NB 0.02 NB 0.02 NO 0.02 ND 0.02 ND 0.02 ND 0.02 NB
IO-2B It A4 A2207 NB 0.02 NB 0.02 NB 0.02 ND 0.02 ND 0.02 NO 0.02 0.03 NB
10-2B B7 A4 A22I4 NB 0.02 NB 0.02 NB 0.02 NO 0.02 NO 0.02 NO 0.02 NB 0.02 ND
10-21 94 At A222t NB 0.02 NB 0.02 ND 0.02 ND 0.02 ND 0.02 NO 0.02 0.02 ND
10-29 ft At A2230 NB 0.02 NB 0.02 NB 0.02 ND 0.02 NB 0.02 NO 0.02 ND 0.02 ND
10-31 9* At A224I NB 0.02 HO 0.02 NB 0.02 NO 0.02 NB 0.02 ND 0.02 ND 0.02 ND
10-31 100 At A2249 ND 0.02 NB 0.02 ND 0.02 NB 0.02 NO 0.02 ND 0.02 NO 0.02 NO
10-31 101 At A2290 NO 0.02 NO 0.02 NO 0.02 ND 0.02 ND 0.02 NO 0.02 ND 0.02 NO
10-31 102 At A2249 1.3 NB 0.02 NB 0.02 ND 0.02 NO 0.02 ND 0.02 0.2B NB
11-
11-
11-
II-
II-
11-
II-
II-
11-
11-
II-
II-
11-
11-
11-
11-
11-
11-
II-
11-
331N A3 A22tl NO 0.02 ND 0.02 NO 0.02 NO 0.02 NO 0.02 ND 0.02 NO 0.02 ND
333E A3 A2270 NB 0.02 ND 0.02 NO 0.02 ND 0.02 ND 0.02 NO 0.02 0.04 NB
lit At A22B2 NB 0.02 NO 0.02 NB 0.02 ND 0.02 NO 0.02 ND 0.02 NO 0.02 ND
117 At A22B1 NO 0.02 ND 0.02 ND 0.02 ND 0.02 NO 0.02 ND 0.02 ND 0.02 ND
IIB At A22BB NB 0.02 NO 0.02 ND 0.02 ND 0.02 NO 0.02 NB 0.02 NB 0.02 NO
119 At A22B7 O.Ot NO 0.02 NB 0.02 ND 0.02 ND 0.02 ND 0.02 0.04 NO
130 At A2302 ND 0.02 NB 0.02 ND 0.02 ND 0.02 ND 0.02 ND 0.02 ND 0.02 ND
132 At A2309 ND 0.02 ND 0.02 ND 0.02 NO 0.02 ND 0.02 ND 0.02 ND 0.02 ND
139 fti A23I3 ND 0.02 ND 0.02 ND 0.02 ND 0.02 NO 0.02 NO 0.02 ND 0.02 NB
NI23 El 19 At A2319 NB 0.02 NO 0.02 ND 0.02 ND 0.02 NO 0.02 ND 0.02 0.04 NB
NI24 El 13 At A23lt 2.1 NO 0.02 NO 0.02 ND 0.02 0.09 ND 0.02 0.9B NB
N129 E123 At 02321 l.t ND 0.02 NB 0.02 ND 0.02 0.07 NB 0.02 O.Ot NB
NI29 EII3 At 02317 NB 0.02 ND 0.02 ND 0.02 NO 0.02 ND 0.02 ND 0.02 ND 0.02 NB
N12t EII9 At A23IB ND 0.02 NB 0.02 NB 0.02 ND 0.02 NO 0.02 NO 0.02 ND 0.02 NB
NI29 El 19 At 02319 NB 0.02 NB 0.02 ND 0.02 NO 0.02 ND 0.02 NO 0.02 0.03 NO
NI29 €125 Ot 02322 0.17 ND 0.02 ND 0.02 ND 0.02 NO 0.02 ND 0.02 0.09 ND
NI2B EI27 Ot 02323 0.19 ND 0.02 ND 0.02 ND 0.02 ND 0.02 ND 0.02 O.I ND
N127 E12B At 02324 0.07 NB 0.02 NB 0.02 NO 0.02 ND 0.02 ND 0.02 0.11 NO
N129 EI30 At 0232t 0.04 NO 0.02 NO 0.02 ND 0.02 ND 0.02 ND 0.02 0.11 ND
HIM C130 At 02327 NB 0.02 NO 0.02 ND 0.02 NO 0.02 ND 0.02 ND 0.02 NO 0.02 NB
11-7 143 At 02337 NB 0,02 ND 0.02 NO 0.02 ND 0.02 ND 0.02 NB 0.02 0.04 NB
11-7 144 At 02343 NB 0.02 NB 0.02 NB 0.02 NO 0.02 NO 0.02 ND 0.02 NO 0.02 ND
11-7 149 At 02342 NB 0.02 ND 0.02 NO 0.02 ND 0.02 NO 0.02 NO 0.02 ND 0.02 ND
11-7 144 At 02341 ND 0.02 NO 0.02 NO 0.02 ND 0.02 ND 0.02 NO 0.02 NB 0.02 NO
-7 47 At 02340 NB 0.02 ND 0.02 ND 0.02 ND 0.02 ND 0.02 ND 0.02 ND 0.02 ND
-7 4B At 02347 NO 0.02 ND 0.02 NO 0.02 NO 0.02 ND 0.02 ND 0.02 ND 0.02 NB
- 0 149 At «393 NO 0.02 ND 0.02 NO 0.02 ND 0.02 ND 0.02 ND 0.02 NO 0.02 ND
-10 30 At 02394 ND 0.02 ND 0.02 ND 0.02 NO 0.02 ND 0.02 ND 0.02 NB 0.02 ND
1-10 91 At «399 ND 0.02 ND 0.02 NO 0.02 ND 0.02 NO 0.02 NO 0.02 ND 0.02 ND
- 0 92 At 0233t ND 0.02 ND 0.02 ND 0.02 ND 0.02 ND 0.02 ND 0.02 ND 0.02 NO
11-10 93 At 023il ND 0.02 ND 0.02 ND 0.02 ND 0.02 ND 0.02 ND 0.02 ND 0.02 N/A
.0 NO
.0 ND
.0 ND
.0 ND
.0 ND
.0 ND
.0 ND
.0 NO
.0 ND
.0 NO
.0 NB
.0 NB
.0 NB
.0 ND
.0 ND
.0 ND
.0 NO
.0 NO
.0 ND
.0 NO
.0 NB
.0 ND
.0 NO
.0 NO
.0 ND
.0 NB
.0 NO
.0 NB
.0 NB
.0 NO
.0 NB
.0 ND
.0 NO
.0 ND
.0 NO
.0 ND
ND
NO
ND
ND
NO
ND
ND
.0 NO
.0 ND
.0 ND
1.0 ND
N/A
.0 ND
.0 ND
.0 ND
.0 NO
.0 ND
.0 ND
.0 HD
.0 ND
.0 NO
.0 ND
.0 ND
.0 NO
.0 ND
.0 ND
.0 ND
.0 NO
.0 NO
.0 ND
.0 NB
.0 ND
.0 ND
.0 NO
.0 ND
.0 NO
.0 ND
.0 ND
.0 ND
.0 ND
.0 ND
.0 ND
.0 ND
.0 ND
.0 ND
.0 ND
.0 ND
.0 NO
.0 ND
.0 ND
.0 NO
.0 ND
.0 NO
.0 ND
.0 NO
.0 ND
.0 ND
.0 NO
.0 NO
N/A
^
.0 ND
.0 NO
.0 NO
.0 ND
.0 NO
.0 NO
.0 ND
.0 ND
.0 NO
.0 NB
.0 ND
.0 NO
.0 HO
.0 NO
.0 ND
.0 ND
.0 NO
.0 NB
.0 NO
.0 NO
.0 NO
.0 NO
.0 ND
.0 ND
.0 ND
.0 ND
.0 NO
.0 ND
.0 ND
.0 ND
.0 ND
.0 ND
.0 ND
.0 NB
.0 NO
.0 ND
.0 ND
.0 NB
.0 NO
.0 NO
NB
ND
ND
ND
NO
ND
I. NO
N/0
«
.0
.0
.0
.0
.0
.0
.0
.0
.0
.0
.0
.0
.0
.0
.0
.0
.0
.0
.0
.0
.0
.0
.0
.0
.0
.0
.0
.0
.0
.0
.0
.0
.0
.0
.0
.0
.0
.0
.0
.0
.0
.0
.0
.0
.0
.0
.0
CanonieEnvircnrnental
Notn ND I dtnottt nan* dittcttd to • levil al I.
-------
TABLE 4
AREAS II,3,4,4,AND 8 EXCAVATION VERIFICATION ANALYSIS
Rfiultt In «g/kg
(Continutd)
H-U
11-11
6«*pl» I.D.
11-10 134 At
11-10 IS9 A4
11-10 134N At
11-10 I37E At
11-10 I33N At
11-10 141 A4
11-11 143 A4
143 At
144 A4
tt-ll 170 At
11-12 171 A4
11-12 334 A3
11-12 331 A3
11-12 341 A3
11-12 342 A3
11-12 343 A3
11-12 344 A3
11-13 34V A3
11-13 332 A3
11-13 333 A3
11-13 334 A3
11-13 333 A3
11-13 334 A3
11-13 331 A3
11-13 340 A3
11-13 341 A3
11-14 344 A3
11-14 347 A3
11-14 341 A3
11-20 3B* A3
11-20 3*0 A3
11-20 391 A3
11-20 3*2 A3
11-23 403 A3
11-23 413 A3
11-29 41* A3
11-23 420 A3
11-24 424 A3
11-24 427 A3
11-24 421 A3
11-21 434 A3
11-21 441 A3
11-21 442 A3
12-1 I43N A3
12-1 I93N A3
12-1 14BN A3
12-1 3*N A3
12-1 14H A3
Lib I.D.
A2342
A23t3
A2344
A2371
A2372
A2373
A2377
A237I
A237*
A2304
A23I*
A23*4
A239I
A240I
A2402
A2403
A240*
A2413
A24II
A24I*
A2420
A2422
A2424
A2423
A2420
A243I
A243*
A244I
A2442
A2444
A244B
A2447
A2471
A24I3
A24V4
A24**
A24*7
A230*
A23IO
A23II
A2320
A2323
A2324
A2343
A2344
A2343
A2342
A233B
1,2-OCB
NO 0.02
NB 0.02
0.24
NO
KB
NB
NB
NB
NB
NB
NB
NB
NB
NB
NB
ND
ND
ND
NO
ND
ND
ND
ND
NB
NB
NB
NO
NB
ND
NB
.02
.02
.02
.02
.02
.02
.02
.02
.1
.02
.2
.2
.2
.02
.02
.02
.02
.02
.02
.02
.02
.02
.02
.02
.02
.02
.02
NB 0.02
NB 0.02
NB 0.02
ND 0.02
ND 0.02
NB 0.02
NB 0.02
NO 0.02
ND 0.02
ND 0.02
ND 0.02
ND 0.02
ND 0.02
ND 0.02
ND 0.02
ND 0.02
2.*
ND 0.02
TRANS 1,1,1-
1,3-DCD 1,4-DCB 1,2-DCE PCE TCA TCE
ND 0.02 ND 0.02 ND 0.02 ND 0.02 ND 0.02 ND 0.02
ND 0.02 ND 0.02 ND 0.02 ND 0.02 ND 0.02 ND 0.02
ND 0.02 ND 0.02 NO 0.02 ND 0.02 ND 0.02 O.It
NB 0.02 NO 0.02 NO 0.02 ND 0.02 NO 0.02 0.13
NB 0.02 NB 0.02 ND 0.02 ND 0.02 ND 0.02 0.04
NO 0.02 ND 0.02 ND 0.02 NO 0.02 NO 0.02 0.01
NB 0.02 ND 0.02 ND 0.02 ND 0.02 NO 0.02 NO 0.02
ND 0.02 ND 0.02 ND 0.02 ND 0.02 NO 0.02 0.02
NB 0.02 ND 0.02 ND .02 ND 0.02 NO 0.02 ND 0.02
NB 0.02 NB 0.02 ND .02 ND 0.02 ND 0.02 0.02
NB 0.02 ND 0.02 ND .02 ND 0.02 ND 0.02 ND 0.02
NB 0.1 NO O.I ND .1 N8 0.1 ND O.I 0.4
ND 0.02 ND 0.02 ND .02 ND 0.02 ND 0.02 ND 0.02
ND 0.2 ND 0.2 ND .2 ND 0.2 ND 0.2 ND 0.2
ND 0.2 ND 0.2 ND .2 ND 0.2 ND 0.2 ND 0.2
ND 0.2 ND 0.2 NO .2 ND 0.2 ND 0.2 ND 0.2
ND 0.02 ND 0.02 ND .02 ND 0.02 HO 0.02 ND 0.02
ND 0.02 ND 0.02 ND 0.02 ND 0.02 NO 0.02 ND 0.02
ND 0.02 NO 0.02 ND 0.02 ND 0.02 ND 0.02 ND 0.02
ND 0.02 ND 0.02 ND 0.02 ND 0.02 NO 0.02 ND 0.02
ND 0.02 ND 0.02 ND 0.02 ND 0.02 ND 0.02 ND 0.02
ND 0.02 ND 0.02 ND 0.02 ND 0.02 NO 0.02 NO 0.02
ND 0.02 ND 0.02 ND 0.02 ND 0.02 ND 0.02 ND 0.02
NO 0.02 ND 0.02 ND 0.02 ND 0.02 ND 0.02 ND 0.02
NO 0.02 ND 0.02 ND 0.02 ND 0.02 ND 0.02 ND 0.02
NO 0.02 NO 0.02 ND 0.02 NO 0.02 ND .02 0.03
ND 0.02 NB 0.02 NB 0.02 NB 0.02 NO .02 NO 0.02
ND 0.02 NB 0.02 ND 0.02 ND 0.02 ND .02 NB 0.02
NB 0.02 NB .02 ND 0.02 NO 0.02 NO .02 ND 0.02
NO 0.02 NB .02 ND 0.02 ND 0.02 ND .02 ND 0.02
ND 0.02 NB .02 ND 0.02 ND 0.02 ND .02 ND 0.02
ND 0.02 NB .02 NB 0.02 NO 0.02 ND .02 ND 0.02
ND 0.02 ND .02 ND 0.02 ND 0.02 ND 0.02 NO 0.02
ND 0.02 ND .02 ND 0.02 ND 0.02 ND 0.02 0.04
ND 0.02 ND .02 ND 0.02 ND 0.02 ND 0.02 ND 0.02
NO 0.02 ND .02 NO 0.02 NO 0.02 ND 0.02 ND 0.02
ND 0.02 ND .02 ND 0.02 ND 0.02 ND 0.02 0.04
ND 0.02 ND .02 ND 0.02 ND 0.02 ND 0.02 ND 0.02
HO 0.02 ND 0.02 NO 0.02 ND 0.02 NO 0.02 ND 0.02
NO 0.02 ND 0.02 ND 0.02 ND 0.02 ND 0.02 ND 0.02
ND 0.02 ND 0.02 ND 0.02 NO 0.02 NO 0.02 0.33
ND 0.02 NO 0.02 ND 0.02 ND 0.02 ND 0.02 ND 0.02
ND 0.02 ND 0.02 ND 0.02 ND 0.02 ND 0.02 ND 0.02
ND 0.02 NO 0.02 NO 0.02 ND 0.02 ND 0.02 0.03
ND 0.02 ND 0.02 ND 0.02 ND 0.02 ND 0.02 ND 0.02
NO 0.02 NO 0.02 NO 0.02 ND 0.02 ND 0.02 ND 0.02
ND 0.02 ND 0.02 ND 0.02 O.I ND 0.02 0.70
ND 0.02 ND 0.02 NO 0.02 ND 0.02 ND 0.02 NO 0.02
Btniin*
N/A
NO .0
ND .0
ND .0
ND .0
ND .0
ND .0
ND .0
ND .0
ND .0
ND .0
ND 3.0
ND 10.0
ND 10.0
ND 10.0
ND 10.0
ND
ND
ND
ND
ND
ND
ND
ND
ND
NO
NO
ND
ND
ND
ND
ND
ND
NO
ND
ND
ND
ND
ND
ND
NO
ND
ND
ND
ND
ND
ND
ND
.0
.0
.0
.0
.0
.0
.
.
.
.
.
.
•
.
•
.
.
.
.0
.0
.0
.0
.0
.0
.0
.0
.0
.0
.0
.0
.0
.0
Ethyl
Dtnitnt
N/A
NO 1.0
ND .0
NO .0
NO .0
NO .0
ND .0
ND .0
ND .0
ND .0
ND .0
ND 3.0
ND 10.0
ND 10.0
ND 10.0
ND 10.0
ND
ND
ND
ND
ND
ND
NO
ND
ND
ND
ND
NB
ND
ND
NO
ND
ND
ND
ND
NO
NO
ND
ND
ND
ND
NO
ND
ND
NO
ND
ND
ND
.0
.0
.0
.0
.0
.0
.0
.0
.0
.0
.0
.0
.0
.0
.0
.0
.0
.0
.0
.0
.0
.0
.0
.0
.0
.0
.0
.0
.0
.0
.0
.0
Toluint
N/A
ND 1.0
ND .0
ND .0
ND .0
ND .0
NB .0
ND .0
NB .0
ND .0
ND .0
ND 9.0
ND 10. 0
ND 10.0
ND 10.0
ND 10.0
ND
ND
NO
ND
ND
ND
ND
NO
ND
ND
ND
ND
ND
NO
ND
ND
ND
ND
ND
ND
NO
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
^
.0
.0
.0
.0
.0
.0
.0
.0
.0
.0
.0
.0
.0
.0
.0
.0
.0
.0
.0
.0
.0
.0
.0
.0
.0
.0
.0
.0
.0
.0
.0
.0
•
lyltnci
N/A
ND .0
ND .0
ND .0
ND .0
NO .0
ND .0
ND .0
ND .0
ND .0
ND .0
13.0
ND 10.0
ND 10.0
ND 10.0
ND 10.0
ND
ND
NO
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
NO
ND
ND
NO
NO
ND
ND
1.*
ND
ND
ND
ND
ND
ND
ND
.0
.0
.0
.0
•
.
.
•
.
.0
.0
.0
.0
.0
.0
.0
.0
.0
.0
.0
.0
.0
.0
.0
.0
.0
3.0
3.0
3.0
ND 1.0
CanonieEnvironmental
Nottt NO I dinotif nont dittcttd to • Itvfl of I.
-------
> o o o o o o oooooo o o o o oooooooooooooooooooooooooo
o
>oooooooo ooooooooooe ooooooooo
'""~"~"""""""""*"o*" *••"•• — — -. _. — ..-...-._. — _ — _.
'SSSSSSSSnSSSSSSSSSSSSSSSSSSSSS
'Oooeoooo ooooooooooo ooooooooo
• •••••••• •••••••••••O*««*a*a>*
ISSSSSSSS-SSSSSSSSSSSSSSSSSSSSS
OOOOOOOOOOOOOOOOOOOO 000000000
••••••••••••••••••••O«***«*B>*
ssssssssssssssssssssssssssssss
S
,000000000000000
oooooooooooooooo
irxcxexNexrxex exexcxex
' O O O O O O O O o O O
ooooooor«ovooooeo<«eooooooo4 rx ex r« ex
oooooo
nw-nooooooKi
O O O O
exrxr4Nexexexcx
oooooooo
ixexexexex
ooooo
fxcxrxexixexex(xcxrx
oooooooooo
OOOOOOoOOO
rxexexcxrxexexcxexiex
excxcxcxexexexexrxrx
oooooooooo
oOOOOOOOOO
U OOOOOOOOOOOOOOOOOOOOOOOOOOOOOOOOOOOOOOOOOOOOOOOO
z ^ dooooooooooooooooooooooooooooooooooooooooooooodd
"- zzzzzzzzzzzzzzzzzzzzzzzzzzzzzzzzzzzzzzzzzzzzzzzz
a exexfxexcxexcxexex(xexexcx.rxcxexcxexexcXMCX.cxi
U OOOOOOOOOOOOOOOOOOOOOOOOOOOOOOOOOOOOOOOOOOOOOOOO
^ dddddddoodoododdodddddododddddddooddddoddddddddd
—' zzzzzzzSzzzSzzzzzzzzzzzzzzzZzzzzzzzZzzSzzzzzzzzz
a NexixexexrxcxcxcxMNMtxexexcxexexexexrxexexrxexextxrxcxrxcxexexcxcxcxcxexexexrxrxfxfxixexexex
U OOOOOOOOOOOOOOOOOOOOOOOOOOOOOOOOOOOOOOOOOOOOOOOO
OOOOOOOOOOOOOOOOOOOOOOOOOOoOOOOOOOoOOOOOOOOOOOOO
ssssssssssssssssssssssssssssssssssssssssssssssss
rx rx rx rx rx rx ex cxcxexcxrxexrxexexcxrxi'xcxexextxexcxexrxexexrxexexcxexexexexexexcxexrxexexexcMex
o o o o o o o oooooooooooooooooooooooooooooooooooooooo
o
«^
f>
cxexexexexcxexcx
xi^lxi^lxi^ixixi^ixixyxBxixir^v^por^r^^f1^^*^^
—••••••«-•#•••.*«-••• ^
wyiWMiyiuriWuiwuiiiJ -Q
X z z Z z
«onp.»_aix->r<<.i i i itxtxrxex — •— — — — fM(M
i i t » i i i i i i i i i i t i i i i i i i i i i i i i i i i i i i i i i i i i i i i i
-------
S-H
• oooooooooooooooooooooooooooooooooooooooooooooo
e ............... • ....... ~'~'~'~'~'~'~'~'~ ......
- ssssssssssssssssssssssssssssssssssssssssssssss
e oooooooooooooooooooooooooooooooooooooooooo
oooo
oooooooooooooooooooooooooooooooooooooooooooooooo
e ooooooooooooooooooo
ooooooooooooooooooooooooo
CM(MCMCMCMCMCMCMCMCMCMCMCMCM(MCM
_ CM _ CM — CM CM CM K)
I I I I I I I I I I I I I I I I I I I I |CJBCJDMaac»O^C^^^^^^«*CMCMCMCMCMCMCMCMCMtMrM
•MCMCMCMCMCMCMCMCMCMfMCMCMCMCMCMCMCMCMCMCMI I I I I I I I ' I I I I I I '^'J^^J.J.^.J.J.J.
-------
TABLE 4
AREAS ID,3,4,i,AND 8 EICAVATION VERIFICATION ANALYSIS
Rnulti in ig/kg
(Continutdl
TRANS 1,1,1- Ethyl
Stcpl* I.D. Lab I.D. 1,2-DCD 1,3-DC( 1,4-DCB 1,2-DCE PCE TCA TCE Otntini Bintina Toluini lyltnn
-27 AB-8 80279 MB 0.02 NB 0.02 NB 0.02 NO 0.02 ND 0.02 NO 0.02 0.02 NO
-27 AB-9 10280 ND
-27 A8-IO B0281 NB
-29 A8-II B031I NB
-2V AB-12 B03I2 NB
-30 A8-I3 10317 NB
-30 A8-14 B03I8 NB
-30 A8-13 B0319 ND
2-2 AB-U 8032* NB
2-2 A8-17 10327 Ml
.02 ND 0.02 ND 0.02 NO 0.02 ND 0.02 ND 0.02 0.03 NO
.02 ND 0.02 NO 0.02 ND 0.02 ND 0.02 ND 0.02 ND 0.02 ND
.02 ND 0.02 ND 0.02 ND 0.02 NO 0.02 ND 0.02 0.02 ND
.02 ND 0.02 NO 0.02 ND 0.02 ND 0.02 NO 0.02 NO 0.02 ND
.02 ND 0.02 NO 0.02 NO 0.02 NO 0.02 NO 0.02 0.04 NO
.02 ND 0.02 ND 0.02 NO 0.02 ND 0.02 NO 0.02 0.04 NO
.02 NO 0.02 ND 0.02 NO 0.02 ND 0.02 NO 0.02 ND 0.02 NO
.02 NO 0.02 ND 0.02 ND 0.02 ND 0.02 ND 0.02 ND 0.02 ND
.02 ND 0.02 ND .02 ND 0.02 ND 0.02 ND 0.02 0.02 NO
2-2 A8-I8 10321 ND 0.02 ND 0.02 ND .02 ND .02 ND 0.02 ND 0.02 0.03 ND
2-2 AB-19 10329 ND 0.02 ND 0.02 ND .02 ND .02 ND 0.02 ND 0.02 0.09 ND
2-2 A8-20 10340 ND 0.02 ND 0.02 ND .02 ND .02 ND 0.02 ND 0.02 0.28 ND
2-3 AB-21 D0348 ND 0.02 ND 0.02 NO .02 ND .02 ND 0.02 ND 0.02 0.02 ND
2-3 AB-22 D034V ND 0.02 ND 0.02 ND .02 NO .02 ND 0.02 ND 0.02 0.02 ND
2-3 AB-23 BOJ30 NB 0.02 ND 0.02 NO 0.02 ND 0.02 ND 0.02 ND 0.02 0.02 ND
2-3 AB-24 B033I NB 0.02 ND 0.02 ND 0.02 ND 0.02 ND 0.02 NO 0.02 NO 0.02 ND
2-3 A4-IB 8033* NO 0.02 ND 0.02 ND 0.02 ND 0.02 ND 0.02 ND 0.02 0.17 NO
2-3 A4-I9 D0337 ND 0.02 ND 0.02 NO 0.02 NO 0.02 NO 0.02 ND 0.02 0.17 ND
2-3 A4-20 B0338 ND 0.02 ND 0.02 ND 0.02 ND 0.02 NO 0.02 ND 0.02 NO 0.02 ND
2-3 NI2B E1I6 At 80369 ND 0.02 ND 0.02 ND 0.02 ND 0.02 ND 0.02 ND 0.02 ND 0.02 NO
.0 ND
.0 ND
.0 ND
.0 NO
.0 ND
.0 NO
.0 NO
.0 ND
.0 ND
.0 ND
.0 ND
.0 ND
.0 NO
.0 ND
.0 NO
.0 ND
.0 ND
.0 ND
.0 ND
.0 ND
.0 NO
.0 ND
.0 ND
.0 NO
.0 ND
.0 ND
.0 ND
.0 NO
.0 ND
.0 NO
.0 NO
.0 ND
.0 NO
.0 NO
.0 ND
.0 ND
.0 ND
.0 ND
.0 ND
.0 NO
.0 NO
.0 ND
.0 ND
.0 ND
.0 ND
.0 ND
.0 ND
.0 NO
.0 ND
.0 ND
.0 NO
.0 NO
.0 ND
.0 ND
.0 NO
.0 ND
.0 ND
.0 ND
.0 ND
.0 ND
.0 NO
.0 ND
.0 ND
.0
.0
.0
.0
.0
.0
.0
.0
.0
.0
.0
.0
.0
.0
.0
.0
.0
.0
.0
.0
.0
Notit NO I dtnottt nont dtttctid to • Itvtl of I.
CanonieEnvironmental
-------
TABLE 5
Sample No.
Al-1
Al-2
Al-3
Al-4
Al-5
Al-6
Al-7
Al-8
Al-9
Al-10
Al-11
Al-12
Al-13
Al-14
Al-15
Al-16
Al-17
Al-18
Al-19
Al-20
EXCAVATION PERIMETER SAMPLE ELEVATIONS
AREA l(a, c)
Sample
Elevation
(Ft) Perimeter
287.0 Vertical
292.0 Lateral
286.0 Vertical
292.0 Lateral
287.0 Vertical
292.0 Lateral
287.0 Vertical
292.0 Lateral
286.0 Vertical
292.0 Lateral
287.0 Vertical
292.0 Lateral
287.0 Vertical
292.0 Lateral
283.5 Lateral
281.0 Vertical
283.5 Vertical
287.0
287.0
287.0
CanonieE
LVironmentc
-------
TABLE 5
EXCAVATION PERIMETER SAMPLE ELEVATIONS
AREA 2
(Continued)
Sample No.
A2-1
*A2-2
A2-3
A2-4
A2-5
A2-6
A2-7
A2-8
A2-9
A2-10
Sample
Elevation
(Ft)
285.5
289.5
286.0
291.5
292.5
286.5
291.5
286.5
291.5
286.0
Perimeter
(NT) Not Tested
Lateral and Vertical
Vertical
Lateral
Vertical
Vertical
Lateral
Vertical
Lateral
Vertical
* Sample taken on sloping ground representing both lateral and vertical
limits of excavation.
CanonieEnvironniental
-------
TABLE 5
EXCAVATION PERIMETER SAMPLE ELEVATIONS
AREA 9
(Continued)
Sample
Elevation
Sample No. (Ft) Perimeter
A9-1 285.5 Lateral
A9-2 282.0 Vertical
A9-3 285.5 Lateral
A9-4 285.5 Lateral
CanonieEnvironmentai
-------
IABLI &
PETKOLEim AREAS EICAVAT10N VERIFICATION ANALYSIS
Sj«plt I.D.
Al-l
AI-2
AI-]
AI-4
AI-3
AI-A
AI-7
Al-B
Al-9
AI-IO
Al II
AI-12
Al IJ
AIM
Al-15
AI-14
AI-17
AI-16
Al 19
AI-70
A2-2
A2 3
A2-4
A2-3
A2-6
A2-7
A2-8
A2 9
A2-10
A9-I
A9-2
A9-3
A9-4
Lab 1.0.
616602
616603
616604
616603
616606
616607
61 6608
616609
414610
616611
616612
616613
418833
618833
B0363
BO 364
B0363
B0366
B0367
B0368
6ISB8I
613082
413883
613884
613883
613886
614331
616332
616333
700936
700997
700938
700939
1,2-OCB
ND 0.02
NO 0.02
NO 0.02
ND 0.02
NO 0.02
NO 0.02
NO 0.02
ND 0.02
NB 0.02
NO 0.02
ND 0.02
NO 0.02
ND 0.02
ND 0.02
NO 0.02
ND 0.02
ND 0.02
ND 0.02
ND 0.02
ND 0.02
NO 0.02
ND 0.02
NO 0.02
NO 0.02
ND 0.02
ND 0.02
ND 0.02
NO 0.02
ND 0.02
NO 0.02
ND 0.02
ND 0.02
NO 0.02
1,3-DCB
ND 0.02
ND 0.02
NO 0.02
ND 0.02
ND 0.02
ND 0.02
NO 0.02
NO 0.02
NO 0.02
ND 0.02
NO 0.02
ND 0.02
ND 0.02
NO 0.02
ND 0.02
ND 0.02
ND 0.02
NO 0.02
ND 0,02
ND 0.02
ND 0.02
ND 0.02
NO 0.02
NO 0.02
ND 0.02
ND 0.02
ND 0.02
NO 0.02
ND 0.02
NO 0.02
ND 0.02
NO 0.02
0.03
1,4-DCB
NO 0.02
ND 0.02
ND 0.02
ND 0.02
NO 0.02
ND 0.02
ND 0.02
ND 0.02
NO 0.02
ND 0.02
NO 0.02
NO 0.02
ND 0.02
NO 0.02
NO 0.02
NO 0.02
ND 0.02
ND 0.02
NO 0.02
NO 0.02
ND 0.02
NO 0.02
NO 0.02
ND 0.02
ND 0.02
ND 0.02
ND 0.02
ND 0.02
NO 0.02
ND 0.02
ND 0.02
NO 0.02
0.02
TRANS
1,2-OCE
ND 0.02
ND 0.02
ND 0.02
ND 0.02
NO 0.02
ND 0.02
ND 0.02
NO 0.02
ND 0.02
ND 0.02
ND 0.02
NO 0.02
ND 0.02
ND 0.02
NO 0.02
NO 0.02
ND 0.02
ND 0.02
ND 0.02
ND 0.02
NO 0.02
ND 0.02
NO 0.02
ND 0.02
NO 0.02
ND 0.02
ND 0.02
NO 0.02
ND 0.02
NO 0.02
ND 0.02
NO 0.02
NO 0.02
PCE
NO 0.02
ND 0.02
ND 0.02
ND 0.02
NO 0.02
ND 0.02
ND 0.02
NO 0.02
ND 0.02
ND 0.02
ND 0.02
NO 0.02
ND 0.02
NO 0.02
ND 0.02
ND 0.02
ND 0.02
NO 0.02
NO 0.02
ND 0.02
ND 0.02
ND 0.02
NO 0.02
NO 0.02
NO 0.02
ND 0.02
NO 0.02
NO 0.02
NO 0.02
NO 0.02
NO 0.02
NO 0.02
ND 0.02
1,1,1-
TCA
NO 0.02
NO O.U2
ND 0.02
ND 0.02
ND 0.02
NO 0.02
NO 0.02
NO 0.02
ND 0.02
NO 0.02
NO 0.02
NO 0.02
ND 0.02
ND 0.02
ND 0.02
NO 0.02
ND 0.02
ND 0.02
ND 0.02
ND 0.02
ND 0.02
ND 0.02
NO 0.02
NO 0.02
ND 0.02
ND 0.02
ND 0.02
ND 0.02
ND 0.02
ND 0.02
ND 0.02
NO 0.02
ND 0.02
TCE
ND 0.02
ND 0.02
ND 0.02
ND 0.02
ND 0.02
ND 0.02
ND 0.02
ND 0.02
NO 0.02
ND 0.02
ND 0.02
0.10
ND 0.02
ND 0.02
ND 0.02
NO 0.02
ND 0.02
ND 0.02
ND 0.02
ND 0.0?
NO 0.02
ND 0.02
NO 0.02
NO 0.02
ND 0.02
ND 0.02
NO 0.02
ND 0.02
ND 0.02
ND 0.02
ND 0.02
ND 0.02
NO 0.02
Benzene
ND 0.2
NO 0.2
NO 0.2
ND 0.2
NO 0.2
ND 0.2
NO 0.2
ND 0.2
ND 0.2
NO 0.2
ND 0.2
NO 0.2
ND 0.2
NO 0.2
ND .0
ND .0
ND .0
ND .0
NO .0
NO .0
ND 0.2
ND 0.2
NO 0.2
ND 0.2
ND 0.2
ND 0.2
ND 0.2
ND 0.2
NO 0.2
ND 0.2
ND 0.2
ND 0.2
NO 0.2
Ethyl
Bentene
ND 0.2
ND 0.2
ND 0.2
ND 0.2
ND 0.2
NO 0.2
ND 0.2
ND 0.2
0.7
ND 0.2
ND 0.2
NO 0.2
ND 0.2
NO 0.2
NO .0
ND .0
ND .0
NO .0
NO .0
ND .0
ND 0.2
ND 0.2
ND 0.2
ND 0.2
ND 0.2
ND 0.2
NO 0.2
ND 0.2
NO 0.2
NO 0.2
ND 0.2
NO 0.2
ND 0.2
Toluene
NO 0.2
NO 0.2
ND 0.2
ND 0.2
NO 0.2
ND 0.2
ND 0.2
NO 0.2
ND 0.2
ND 0.2
NO 0.2
ND 0.2
ND 0.2
NO 0.2
ND .0
NO .0
ND .0
ND .0
ND .0
NO .0
NO 0.2
ND 0.2
ND 0.2
ND 0.2
NO 0.2
ND 0.2
NO 0.2
ND 0.2
ND 0.2
ND 0.2
ND 0.2
NO 0.2
ND 0.2
lylenes
0.2
NO 0.2
NO 0.2
NO 0.2
ND 0.2
NO 0.2
ND 0.2
NO 0.2
4.1
ND 0.2
NO 0.2
ND 0.2
ND 0.2
ND 0.2
NO .0
ND .0
ND .0
NO .0
ND .0
ND .0
ND 0.2
ND 0.2
NO 0.2
ND 0.2
ND 0.2
ND 0.2
ND 0.2
NO 0.2
0.2
ND 0.2
NO 0.2
ND 0.2
ND 0.2
Nottt NO 1 dtnotet none detected to • level o« X.
CanonieEnvircnmental
-------
TABLE 6
PETROLEUM AREAS EXCAVATION VERIFICATION ANALYSIS
Results in •g/fcg
(Continued)
Siiplt
Al-1
AI-2
Al-3
AI-4
Al-S
AI-6
Al-7
AI-8
Al-»
Al-IO
Al-lt
AI-12
Al-13
AI-14
Al-15
AI-16
AI-17
AI-IB
Al-19
AI-20
A2-2
A2-3
A2-4
A2-3
A2-6
A2-7
A2-8
A2-9
A2-10
A9-1
A9-2
A9-3
A9-4
Notts:
1.0. Lib I.D.
616602
616603
616604
616609
616606
616607
61660B
616609
616610
616611
616612
616613
618855
6IB8S5
B0363
619140
B036S
619141
619142
619143
615881
615882
615883
615884
613865
61 5886
616331
616332
616333
700956
700957
700958
7009S9
l.NT denotes
Trichloro-
Uuoro«»th»ne
0.04
0.03
0.03
0.03
NO 0.02
NO 0.02
0.04
NO 0.02
ND0.02
0.06
0.03
NO 0.02
ND 0.02
NO 0.02
NT
NT
NT
NT
NT
NT
0.29
0.22
0.03
NO 0.02
0. 12
0.22
ND 0.02
ND 0.02
0. 10
ND 0.02
0.02
0.25
0.14
"not tested".
2.ND II denotes none detected
3. The non-detectable lints
Arsenic
B»r iu«
Cadaiu*
Chrociu* (Total)
Hercury
Lead
Sel em u«
Si 1 ver
Nethylene
CMorid*
NO 0.02
ND 0.02
NO 0.02
ND 0.02
ND 0.02
NO 0.02
ND 0.02
ND 0.02
ND 0.02
ND 0.02
ND 0,02
ND 0.02
NO 0.02
NO 0.02
NT
NT
NT
NT
NT
NT
0.04
0.07
ND 0.02
ND 0.02
NO 0.02
ND 0.02
ND 0.02
NO 0.02
ND 0.02
NO 0.02
ND 0.02
NO 0.02
ND 0.02
to t level
EP Toxic
Me tils
NT
ND
ND
ND
NT
NO
ND
ND
NT
ND
ND
ND
NT
NT
NT
NO
NT
ND
ND
ND
ND
NT
ND
NT
NT
ND
ND
NO
ND
NT
ND
ND
NT
of X.
PCB
NT
ND
NT
ND
ND
ND
NT
ND
NT
ND
NT
ND
NT
NT
NT
ND
NT
ND
ND
ND
ND
NT
ND
ND
NT
ND
NT
NO
ND
ND
ND
ND
ND
1242
0.1
0.1
0. 1
0.1
U.I
O.I
0.1
0.2
0. I
0. 1
0. 1
0. 1
0.1
0.1
0. 1
0.1
0.1
0.001
0.001
0.001
0.01
PCB
NT
ND
NT
ND
ND
ND
NT
ND
NT
ND
NT
ND
NT
NT
NT
ND
NT
ND
ND
NO
NO
NT
ND
ND
NT
ND
NT
NO
ND
NO
ND
ND
1254
0. I
O.I
0. 1
0. 1
O.I
O.t
U. 1
0. 1
0. 1
0. 1
0. 1
0. I
0.1
0. 1
(). 1
0. 1
0. 1
0.001
0.001
0.001
0.002
for EP Toxicity Metils are listed
ND 0.5
ND lu.u
ND 0. 10
NO i.i.5
ND u.u2
NO '1.5
ND H. i
ND U.5
below
PCB
NT
NO
NT
NO
ND
NO
NT
NO
NT
ND
NT
1260
0.1
O.I
('. 1
0.1
0. 1
0. 1
0. 14
NT
NT
NT
ND
NT
ND
ND
ND
NO
NT
ND
NO
NT
NO
NT
NO
ND
ND
ND
NO
ND
.
0. 1
0. 1
u. 1
0.1
0. 1
0.1
0.2
0. 1
0. 1
0.1
0.001
0.001
0.001
0.001
i
TEH
24.0
97.0
ND 10.0
ND 10.0
ND 10.0
ND 10.0
ND 10.0
ND 10.0
610.0
81.0
21.0
110.0
ND 10. U
NO 10.0
NT
8.0
NT
2800.0
17d.O
36.0
NT
ND 10.0
NT
NT
ND 10.0
NT
ND 75.0
ND 16.0
ND 17.0
20.0
11.0
ND 10.0
970. U
fiJM
CanonieEnvironmental
-------
TABLE 6
PETROLEUM AREA EXCAVATION VERIFICATION ANALYSIS
Results in ug/kg
(Continued)
Nitrobenzene Phenant^rene Acenapthene Fluoranthene Pvrene Fluorene Anthracine bis (-2-Chloroethoxv)
2 1,900.0 460.0 1,000.0 460.0 1,000.0
*Al-9 600.0
Al-10 330.0 640.0
*A1-12 580.0 1,100.0 710.0
Al-18 720.0
Note: Samples Al-1 through Al-20, A2-2 through A2-10, and A9-1 through A9-4 analyzed
for acid/base neutrals by U.S. EPA Method 8270 contained concentrations less
than the detection limit for each chemical constituent analyzed, with
the exception of these listed above. Samples Al-15 and Al-17 were not
tested. The detection limits for all of the chemical constituents tested
by Method 8270 are shown on the following two pages.
*Additional soils were excavated around these sampling points.
CanonieEnviroimenial
-------
TABLE 6
PETROLEUM AREA EXCAVATION VERIFICATION ANALYSIS
GC/MS
SEMI-UOLATILE ANALYSIS
COMPOUND NAME
AMOUNT
N-Nitrosodimethylamine
Phenol
bis(-2-Chloroethyl)Ether
2-Chloroohenol
1 ,3-Dichlorobenzene
1 .4-Dichlorobenzene
1 ,2-Dichlorobenzene
bi9(2-chloroi*ooroDyl)Ether
N-Nitroso-Di-Prooylamme
Hexach loroethane
N 1t robenzene
I soohorone
2-Nit rooheno1
2 .4-Dimethylohenol
bis(-2-Chloroethoxy)nethane
2 ,4-DichloroDhenol
1 .2 ,4-Trichlorobenzene
Naphthalene
Hexachlorobutadiene
4-Chloro-3-Methylphenol
Hexachlorocyclooentadiene
2,4.6-TrichloroDhenol
2-Chloronaohthalene
Dimethyl Phthalate
Acenaohthylene
2,6-Dinitrotoluene
Acenaohthene
2.4-Dinitroohenol
4-Nit rooheno 1
2.4-Dinitrotoluene
Diethylohthalate
4-Chlorophenyl-phenylether
Fluorene
Benz id me
4.6-Dinitro-2-Methylohenol
N-Nitrosodiohenylamina
4-Bromoohenyl-Dhenylether
Hexach lorobenzene
Pentachloroohenol
Phenanthrene
Anthracene
Di-N-Butylohthalate
F luoranthene
DET. LIMIT
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
NO
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
330
330
330
330
330
330
330
330
330
330
330
330
330
330
330
330
330
330
330
330
330
330
330
330
330
330
330
1650
330
330
330
330
330
330
1650
330
330
330
1650
330
330
330
330
ug/Kg
ug-'Kg
ug/Kg
ug/Kg
ug-'Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Ko
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
UQ/KO.
CanonieEnvironmental
-------
TABLE 6
PETROLEUM AREA EXCAVATION VERIFICATION ANALYSIS
(CONTINUED)
GC/MS
SEMI-VOLATILE ANALYSIS
COMPOUND NAME
Pyrcne
Butylbenzylohthalate
3.3'-Dichlorobenzidine
Benzo(a)Anthracene
bis-(2-Ethylhexyl)Phthalate
Chrysene
Di-N-Octyl Phthalate
Benzo(b)Fluoranthene
Benzo(k)Fluoranthene
Benzo(a)Pyrene
IndenoCl.2.3-cd)Pyrene
Dibenzo(a.h)Anthracene
Benzo(Q,h,i)Pervlene
AMOUNT
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
DET. LIMIT
370
330
660
330
330
330
330
330
330
330
330
330
330
ug/Kg
ug/Kg
tig/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ua/Ka
CanonieEnvironmentdi
-------
TABLE 7
SUMMARY OF PETROLEUM AREA SOILS AERATION
Date
Pilot Study
3/16/87
3/17/87
3/18/87
3/19/87
3/20/87
3/23/87
3/24/87
3/25/87
3/26/87
3/27/87
3/30/87
3/31/87
4/01/87
4/02/87
4/03/87
4/06/87
4/07/87
4/08/87
4/09/87
4/10/87
4/13/87
4/14/87
4/15/87
4/16/87
4/17/87
TOTALS
No. of
Mixer Loads
30
3
15
16
17
15
15
16
18
15
18
15
0
0
17
18
0
12
14
14
16
16
15
16
18
16
365
Original No.
of GC/MS
Samples Taken
6
1
2
1
2
1
2
1
2
2
2
1
0
0
2
2
0
1
2
2
1
2
2
2
2
_1
42
Dilution
"Oily" vs. "Clean"
5/3
5/3
5/3
2/1
7/3
7/3
2/1
2/1
2/1
3/2
3/2
3/2
0
0
3/2
3/2
0
3/2
3/2
3/2
3/2
3/2
3/2
3/2
3/2
3/2
_
Oily Soils
Processed
(Bulk Yd3)
150
15
75
85
95
84
80
85
95
72
86
72
0
0
82
86
0
58
67
67
77
77
72
77
86
77
1,820
Make-up
Soils Processed
(Yd3)
79
8
39
37
36
32
35
37
42
42
50
42
0
0
48
50
0
34
39
39
45
45
42
45
50
45
961
CanonieEnvironment
.a;
-------
TABLE 8
SUMMARY OF PETROLEUM AREA SOILS AERATION
POST-TREATMENT ANALYTICAL RESULTS
Analyte
Naphthalene
Acenapthylene
Acenaphthene
Fluorene
Phenanthrene
Anthracene
Fluoranthene
Pyrene
Benzo(a) Anthracene <330 <234
Chrysene <330 <256
TEH - 30
Date of Aeration
Average Concentration of Samples (ppb)
3/16 3/17 3/18 3/19 3/20 3/23 3/24 3/25 3/26 3/27
<330 <306 <170 <170 <330 <170 <330 <330 <170 <330
<330 <234 <170 <170 <330 <170 <330 <330 <170 <330
<330 <234 <170 <170 <330 <170 <330 <330 <170 <330
<330 <234 <170 <170 <330 <170 <330 <330 <170 <330
400 <418 590 580 <330 435 460 585 255 <555
<330 <234 230 <175 <330 <225 <330
<330 <432 <500 <500 <330 <500 <330
<330 <500 <330 <370 <330 <345 510
170 190 <330 210 <330
300 245 <330 260 <330
47 < 42 58 < 15 55
<330 275 975
380 <500 <440
615 <330 630
<330 <170 <620
<330 <170 <595
44 18 34
Note: PAH concentrations given in ppb
TEH concentrations given in ppm
CanonieEnvironmenta'.
-------
TABLE 8
SUMMARY OF PETROLEUM AREA SOILS AERATION
POST-TREATMENT ANALYTICAL RESULTS
(Continued)
Analyte
Naphthalene
Acenapthylene
Acenaphthene
Fluorene
Phenanthrene
Anthracene
Fluoranthene
Pyrene
Benzo(a) Anthracene
irysene
TEH
Average Cone
3/30
<330
<330
<330
<330
440
480
<330
624
<330
<330
34
4/2
< 570
< 497
< 497
< 497
<1355
< 547
<1493
<1012
< 497
< 497
195
4/3
<330
<330
<330
<330
810
<380
<990
<660
<330
<330
190
4/7
<330
<330
<330
<330
830
500
<990
<660
<330
<330
150
4/8
<330
<330
<330
<330
1180
<495
<990
<660
<330
<330
225
4/9
<330
<330
<330
<330
1650
<330
<990
760
<330
<330
285
Date of Aeration
Concentration of Samples (ppb)
4/10 4/13 4/14 4/15 4/16 4/17
<170 <330 <170 <170 <170 <660
<170 <330 <170 <170 <170 <660
<170 <330 <170 <170 <170 <660
<170 <330 <240 <300 <330 <660
810 1275 1600 1850 1800 2500
<300 <330 <170 <260 <215 <660
<500 <990 <500 <580 <500 <2000
450 <660 525 705 610 <1300
<170 <330 360 420 390 <660
<170 <330 390 <170 495 <660
130 140 158 155 175 140
Note: PAH concentrations given in ppb
TEH concentrations given in ppm
CanonieEnvironmentdl
-------
TABLE 9
COST BREAKDOWN FOR AERATION OF
AREA 1(8), 3, 4, 6, AND 8
Item Cost
Salaries and Wages $405,450
Rental 596,250
Supplies 453,150
Subcontracts • 620,100
Fuel 47,700
Other Professional Services 262.350
TOTAL $2,385,000
Note: This cost does not include mobilization, site characterization,
pilot study, site closure, disposal of waste materials, and
demobilization.
CanonieEnvircnmentdi
-------
TABLE 10
COST BREAKDOWN FOR AERATION OF
AREAS l(a, c), 2, AND 9
Item Cost
Salaries and Wages $ 88,910
Rental 130,880
Supplies 93,370
Subcontracts 135,980
Fuel 10,460
Other Professional Services 57.530
TOTAL $517,130
Note: This cost does not Include site characterization, pilot study, or
demobilization.
CanonieEnvircnmental
-------
TABLE 11
SUMMARY OF SOIL VOLUMES EXCAVATED AND TREATED
Area Cubic Yards
1(A,C) 900
1(B) 605
2 800
3 5,290
4 530
6 1,731
8 1,250
9 200
Lagoon 150
CanonioEnvircnmental
-------
REVISIONS
:f DRAWN _ JYA__ CHUCKED BV
[ BY 5-14-87 APPROVED Br
DRAWING
~5 I 7 -it Vi71 NUMBER
I
1 -!
i\
r
O ,. 'm
-------
REVISIONS
NO.
DATF
DRAWN
BY
JVA
J-26-87
CHECKED BY
APPROVED BY
TKK
P MIK
1 !- *T7
> n <*!
DRAWING _uo .. r
NUMBER CH84— 130— E86
>
1/1
-------
REVISIONS
NO.
DATE
DRAWN
BY
JVA
6-20-87
CHECKED BY
APPROVED BY
TV H
Flff
1 I ftT
7 n H?
N5SCH84-130-E93
'0.000
'0.050
U1O
Cn
o
o
§
o
z
Ol
N)
CD
O
o
X
PI o
i> m
H "D
m o
-------
REVISIONS
NO
DATE
DRAWN
BY
JVA
6-7-87
CHECKED BY
APPROVED BY
~T*H
RMK
7-1 *1
7 ZJ-&7
DRAWING _, I0 . . -.n .-_,
NUMBER CH84-130-E91
F 10 060 0
>
I/I
;2<
o
T)
m
3 >
-------
REVISIONS
NO
DATE
DRAWN
BY
JVA
6-7-87
CHECKED BY
APPROVED BY
TKK
PMB
1- 1 • 1 1
7 21 87
R5KCH84-130-E90
5 >
^ 33
» n ;
-------
REVISIONS
DRAWN
BY
JVA
CHECKED BY
6-20-87 APPROVED BY
-l i »7 DRAWING -u- . ,n __„
/ /I ••/ NUMBER CH84-150-E92
^
!?
i op
2 >
-------
REVISIONS
NO
DATE
DRAWN
BY
JVA
3-17-87
CHECKED BY
APPROVED BY
TnW
P/Mg
l-l ft -i
^ / ,-7
KGCH84-130-E85
-t 9.9000
-------
REASONS (^j
DRAWN
BY
JVA
3-17-87
CHECKED BY
APPROVED BY
1 . I-
b/»> e
~ •*< ' •
7 JJ fl?
DRAWING., Q
NUMBER CH84- 130-E82
-E 9.9000
-E 9,9500
-E 10.0000
O
o
-------
REVISIONS
NO. 1
DATE] ,
DRAWN
BY
JVA
3-17-87
CHECKED BY
APPROVED BY
DRAWING _,,„. _ .-0,
NUMBER CH84-130-E81
E 9,900 0
E 9.9500
E 10,000
p
b
to
o
p
b
o
o
-------
(SEVISIONS
NO 1
DATE! r
DRAWN
BY
JVA
3-17-87
CHECKED BY
APPROVED BY
TKH
KVnF-
1 1 -r
r /; •-, /
jRAWING^up. , -,n rnA
NUMBER CH84 130 E84
E '0.500
c
m
D * *: ** F
— " Is
-------
REVISIONS
NO. 1
DATE]
DRAWN
BY
JVA
3-16-87
CHECKED BY
APPROVED BY
Ring
J. z i f, J
DRAWING „,,„. . ,_ ,_or.
NUMBER CH84-130-E80
'0,000.0
'0.0500
'0.1000
'0.1500
S S
§ S S
z
en
p
b
-a
m
8
b
Ol
N)
Ol
o
o
s
b
m
m
o
o
O
n &
'--- ' "
-------
APPENDIX C
LABORATORY ANALYTICAL REPORTS -
PETROLEUM AREA SOIL AERATION -
U.S. EPA METHOD 8270 AND
TOTAL EXTRACTABLE HYDROCARBONS
CanonieEnvironmer.t
-------
Revised Report
Client ID: MCKIN
Samole ID: 84-130-1640
Matrix : SOIL
SAMPLE 3-16-2
Data
3981
File:>B2286
702286
GC/MS
SEMI-VOLATILE ANALYSIS
C-l
COMPOUND NAME
AMOUNT
DET. LIMIT
N-Nitrosodimethylamine
Pheno1
bis(-2-Chloroetnyl)Ether
2-Chlorophenol
1.3-Dichlorobenzene
1,4-Dichlorobenzene
1,2-Dichlorobenzene
bis<2-chloroisopropyl)Ether
N-Nitroso-Di-Propylamine
Hexachloroethane
Nit robenzene
Isophorone
2-Ni t ropheno1
2,4-DimethyIpheno1
bis(-2-Ch1oroethoxy)Methane
2,4-Dichlorooheno1
1.2.4-Trichlorobenzene
Naphthalene
Hexachlorobutadiene
4-Chloro-3-MethyIpheno1
Hexachlorocyclopentadiene
2,4.6-Trichlorophenol
2-Chloronaphthalene
Dimethyl Phthalate
Acenaphthylene
2,6-Dinitrotoluene
Acenaohthene
2,4-Din itropheno1
4-Nit ropheno1
2,4-Dinitrotoluene
Diethylphthalate
4-Chloropheny1-phenylether
Fluorene
Benzidine
4,6-Din i tro-2-MethyIpheno1
N-Nitrosodiphenylamine
4-Bromopheny1-phenylether
Hexach lorobenzene
Pentachloropheno1
Phenanthrene
Anthracene
Di-N-Butylohthalate
Fluoranthene
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
400.
ND
NO
ND
330
330
330
330
330
330
330
330
330
330
330
330
330
330
330
330
330
330
330
330
330
330
330
330
330
330
330
1650
330
330
330
330
330
330
1650
330
330
330
1650
330
330
330
330
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
UQ/KQ
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
UQ/KQ
CanonleEnviraimentdi
-------
REVISIONS
NO.
DATF
DRAWN
BY [3^T7-87.
JVA
CHECKED BY
APPROVED BY
DRAWING- _
i .1 ^[NUMBER CH84-150-
'0.000
OI
8
o
tn
i
o
NJ
C/l
p
O
~! O
-------
CO
LJ
I
O
T
CO
I
O
"a:
1-3 1-46
1-42 1-47
1-43 1-48
N 5.0500
LEGEN
a f<
NOTf
AREA 1P
PERIMETER
Canont
DATE 3-17-67
I SCALE AS SHOWN
-------
REVISIONS
j: DRAWN
I BY
JVA I CHECKED BY
3-23-87 I APPROVED BY
T I
i-9,?
DRAWING rup.- .~~. cao
NUMBER CH84-I3O-EB8
f"fi
8=1
!i
I
i i
D
-------
APPENDIX A
MISCELLANEOUS LABORATORY
ANALYTICAL REPORTS
CanonieEnvironmentaJ
-------
Table 1
Codes of Samples Received
From McKin
Project: 84-130
05-21-1987
84-130-2134
Page 1
Date
Sampler JJ) Sampled
Analysis: Purgeable Aromatics
Oecon Water 05-12-87
Analysis: Purgeable Halocarbons
Oecon Water 05-12-87
Date
Received
05-13-87
05-13-87
Lab ID|
705934
705935
705936
705934
705935
705936
Water
Water
Water
Water
Water
Water
Container
40 ml vial
40 ml vial
40 ml vial
40 ml vial
40 ml vial
40 ml vial
CanonieEnvironmental
-------
Note:
Tab.e 2 05-21-1987
Results of Purgeable Aromatics Analysis on Water 84-130-2134
Samples Received From McKin Page 2
Results In mg/1
Sampler ID: Decon
Water
Lab 101: 705934
Analyte(s)
Benzene NO 0.05
Chlorobenzene ND 0.05
1,2-Dichlorobenzene ND 0.05
1,3-Dlchlorobenzene ND 0.05
1.4-Oichlorobenzene ND 0.05
Ethylbenzene ND 0.05
Toluene ND 0.05
Xylene 0.11
M.
Analyst Checked by
ND x'denotes none detected to a level of X. CanOIU0EnvirOnmental
-------
Tab.c 3
Results of Purgeable Halocarbons Analysis on Water
Samples Received From McKln
Results In mg/1
05-21-1987
84-130-2134
Page 3
Sampler ID:
Lab IDI:
Analyte(s)
Bromodlchloromethane
Brorooform
Bromomethane
Carbon tetrachloride
Chlorobenzene
Chloroethane
2-Chloroethylvinyl ether
Chloroform
Chloromethane
Dlbromochloromethane
1,2-Oichlorobenzene
1.3-Dichlorobenzene
1,4-Dlchlorobenzene
Dlchlorodlfluoromethane
1.l-0lchloroethane
1,2-Dichloroethane
1,1-Dlchloroethene
trans-1.2-Dlchloroethene
1,2-Dichloropropane
c1s-1,3-01chloropropene
trans-1,3-Di chloropropene
1.1,2.2-Tetrachloroethane
Tetrachloroethene
1,1,1-Trlchloroethane
1,1,2-Trlchloroethane
Trlchloroethene
Trlchlorofluoromethane
Vinyl chloride
Methylene chloride
NO
NO
Oecon
Water
705934
NO 0.005
NO 0.005
NO 0.005
NO 0.005
NO 0.005
NO 0.005
0.005
0.005
NO 0.005
NO 0.005
0.011
NO 0.005
NO 0.005
NO 0.005
NO 0.005
NO 0.005
NO 0.005
NO 0.005
NO 0.005
NO 0.005
NO 0.005
NO 0.005
0.005
NO
NO 0.005
NO 0.005
0.015
NO 0.005
NO 0.005
NO 0.005
Analyst Checked by
CanonieEnvironmental
-------
Client IP:
Sample ID:
Matrix :
MCWIN
84-130-2134
WATER
SAMPLE- DECON WATER
Data
File:
705937
GC/MS
SEMI-VOLATILE ANALYSIS
A-4
COMPOUND NAME
AMOUNT
DET. LIMIT"
N-Nit rosodimethylamine
Phenol
bis<-2-Chloroethyl)Ether
2-Chlorophenol
1 ,3-Dichlorobenzene
1,4-Dichlorobenzene
1,2-Dich1orobenzene
bis(.2-chloroisopropyl )Ether
.N-Nitroso-Di-Propylamine
Hexachloroethane
Nit robenzene
Isopho rone
2-Nit ropheno1
2 ,4-Dimethylphenol
bis(-2-Chloroethoxy)Me thane
2 ,4-Dichlorophenol
1,2,4-Trichlorobenzene
Naphtha lene
Hexachlorobutadiene
4-Chloro-3-Methylphenol
Hexachlorocyclopentadlene
2,4,6-Trichloroohenol
2-Chloronaphthalene
Dimethyl Phthalate
Acenaphthylene
2 ,6-Dinitrotoluene
Acenaphthene
2 ,4-Dinitrophenol
4-Nit ropheno1
2,4-Dinitrotoluene
Diethylphthalate
4-Chlorophenyl-phenylether
F luorene
Benzid ine
4,6-Dinitro-2-Methylphenol
N-Nit rosodiphenylamine
4-Bromophenyl-phenylether
Hexach lorobenzene
Pentach loropheno 1
Phenanthrene
Anthracene
Di-N-Butylphthalate
Fluoranthene
ND
1800.
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
100.
ND
ND
ND
NO
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
100
100
100
100
100
100
100
100
100
100
100
100
ioa
100
100
100
100
100
100
100
100
100
100
100
100
100
100
500
100
100
100
100
100
100
500
100
100
100
500
100
100
100
100
ug/L
ug/L
uq/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug'L
ug/L
uq/L
ug/L
ug 'L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug 'L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
CanonieEnvironmentai
-------
A-5
MCKIN
705937
PAGE 2
LP-2134
Pyrene
ButyIbenzylphthalate
3,3'-Dichlorobenzidine
Benzo ' a ) Anthracene
bis-(2-Ethylhexyl)Phthalate
Chrysene
Di-N-Oetyl Phthalate
Benzo(b)Fluoranthene
Benzo'k)Fluoranthene
Benzo
-------
Tab. 2
Results of Polynuclear Aromatlcs Analysis on Water
Samples Received From McKln
Results in mg/1
03-30-1987
84-130-1867
Page 2
Sampler ID:
Lab IDI:
Analyte(s)
Acenaphthene
Acenaphthylene
Anthracene
Benzo (a) anthracene
Benzo (a) pyrene
Benzo (b) fluoranthene
Benzo (ghl) perylene
Benzo (k) fluroanthene
Chrysene
Dlbenzo (a,h) anthracene
Fluoranthene
Fluorene
Indeno (1,2.3-cd) pyrene
Naphthalene
Phenanthrene
Pyrene
CarbonBed
Condensate
702564
NO 0.05
NO 0.05
NO 0.05
NO 0.05
NO 0.05
ND 0.05
NO 0.05
NO 0.05
ND 0.05
ND 0.05
ND 0.05
ND 0.05
ND 0.05
IND 0.5
ND 0.05
ND 0.05
Analyst Checked by
Note:
ND X denotes none detected to a level of X.
r ^ »r, •intavf airinn
CanomeEnvironmental
-------
Cliant ID:
Sample ID:
Ma t r i x :
MCKIN
84-130-1867
UATER
SAMPLE- CONDENSATE
Data Ft la:>B2564
702564
GC/MS
SEMI-VOLATILE ANALYSIS
A-7
COMPOUND NAME
AMOUNT
DET. LIMIT
N-Ni t r o sod i me thy lam me
Phenol
bis(-2-Chloroethyl)Ether
2-Chloroohenol
1.3-Dichlorobenzene
1,4-Dichlorobenzene
1.2-Dichlorobenzene
bis(2-ch loroisooropylJEther
N-Ni troso-Di-Propylamme
Hexach loroethane
Ni t robenzene
Isophorone
2-Ni t ropheno1
2,4-Dimethylphenol
bis(-2-Chloroethoxy)Methane
2,4-Dichloroohenol
1.2,4-Trichlorobenzene
Naphthalene
Hexachlorobutadiene
4-Chloro-3-Methylphenol
Hexachlorocvclopentadiene
2,4,6-Trichloropheno1
2-Chloronaphthalene
Dimethyl Phthalate
Acenaphthylene
2,6-Dinitrotoluena
Acenaphthene
2,4-0in i tropheno1
4-Ni t ropheno1
2.4-Dinitrotoluena
Diethylphthalate
4-Chloropheny1-phenylather
Fluorene
Benzidine
4,6-Dini tro-2-Methylpheno 1
N-Nitrosodiphenylamin*
4-Bromopheny1-pheny1 ether
Hexach lorobenzene
Pentach loropheno1
Phenanthrene
Anthracene
Di-N-Butylphthalate
Fluoranthene
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
NO
ND
ND
40
40
40
40
40
40
40
40
40
40
40
40
40
40
40
40
40
40
40
40
40
40
40
40
40
40
40
200
40
40
40
40
40
40
200
40
40
40
200
40
40
40
40
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
UQ/L
CanonleEnvircnmental
-------
A-3
MCKIN
702564
PAGE 2
LP-1867
Pyrene
Butylbenzylphthalate
3,3'-Dichlorobanz id ine
Benzo(a)Anthracene
bis-(2-Ethylhexyl)Phthai ate
Chrysena
Di-N-Octyl Phthalate
Benzo(b)Fluoranthane
Benzo(k)Fluoranthane
Benzo(a)Pyrene
Indenod .2 ,3-cd )Pyrene
Dibenzo(a.h)Anthracene
Benzo(a .h.i)Pervlene
ND
NO
MO
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
40
40
80
40
40
40
40
40
40
40
40
40
40
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ua/L
Ana 1vst
Checked Bv
CanonieEnvircnmentdl
-------
Tab,. 2
Results of Polynuclear Aromatlcs Analysis on Water
Samples Received From McKin
Results in mg/1
03-11-1987
84-130-1743
Page 2
Sampler 10:
Lab IDI:
Analyte(s)
Acenaphthene
Acenaphthylene
Anthracene
Benzo (a) anthracene
Benzo (a) pyrene
Benzo (b) fluoranthene
Benzo (ghi) perylene
Benzo (k) fluroanthene
Chrysene
Dlbenzo (a,h) anthracene
Fluoranthene
Fluorene
Indeno (1,2,3-cd) pyrene
Naphthalene
Phenanthrene
Pyrene
Well 18-A
701036
ND 0.01
ND 0.01
ND 0.01
ND 0.01
ND 0.01
ND 0.01
ND 0.01
ND 0.01
ND 0.01
ND 0.01
ND 0.01
ND 0.01
ND 0.01
ND 0.01
ND 0.01
ND 0.01
Analyst Checked by
Note:
ND X denotes none detected to a level of X.
CanonieEnvironmental
-------
Table 3 03-11-1987
Results of Purgeable Aromatics Analysis on Water 84-130-1743
Samples Received From McKln page 3
Results in mg/1
Sampler 10: Well 18-A
Lab ID*: 701036
Analyte(s)
Benzene NO 0.05
Chlorobenzene NO 0.05
1,2-01Chlorobenzene NO 0.05
1,3-01Chlorobenzene NO 0.05
1.4-0lchlorobenzene NO 0.05
Ethylbenzene NO 0.05
Toluene NO. 0.05
Xylene NO 0.05
__
Analyst Checked
N?1" — , u CanonieEnvironmental
V An^^tnr' nnn/> An*t*r-taf\ tf\ » louol flf
-------
Results of Purgeable Halocarbons Analysis on Water
Samples Received From McKin
Results in mg/1
03-11-1987
84-130-1743
Page 4
Sampler 10:
Lab 101:
Analyte(s)
Bromodichloromethane
Bromoform
Brofflonethane
Carbon tetrachloride
Chlorobenzene
Chloroethane
2-Chloroethylvinyl ether
Chloroform
Chloromethane
Oibromochloromethane
1,2-Oichlorobenzene
1,3-Dichlorobenzene
1,4-Dichlorobenzene
Oichlorodifluoromethane
1,1-Oichloroethane
1,2-Di chloroethane
1,1-Dichloroethene
trans-1.2-Dichloroethene
1.2-Oichloropropane
cis-1,3-01chloropropene
trans-1,3-Dichloropropene
1.1,2,2-Tetrachloroethane
Tetrachloroethene
1,1,1-Trichloroethane
1.1,2-Trlchloroethane
Trichloroethene
Trichlorofluoromethane
Vinyl chloride
Methylene chloride
Well 18-A
701036
NO 0.005
NO 0.005
NO 0.005
NO 0.005
NO 0.005
NO 0.005
NO 0.005
NO 0.005
NO 0.005
NO 0.005
NO 0.005
NO 0.005
NO 0.005
NO 0.005
NO 0.005
NO 0.005
NO 0.005
NO 0.005
NO 0.005
NO 0.005
NO 0.005
NO 0.005
NO 0.005
0.19
NO 0.005
NO 0.005
NO 0.005
NO 0.005
NO 0.005
__
Analyst Checked by
CanonieEnvironmental
-------
Table 5
Results of Total Ext. Hydrocarbons Analysis on Water
Samples Received From McKin
Results In mg/1
03-11-1987
84-130-1743
Page 5
Sampler ID:
Lab ID!:
Analyte(s)
Total Extractable Hydrocarbons
Well 18-A
701036
NO 1.0
JftL
Analyst Checked by
Note:
tin v
in » lauol nf X.
CanonieEnvironmenta}
ISJ
-------
Client 10:
Sample ID:
Matrix :
MCKIN
84-130-1840
WATER
Data File:>B2292
SAMPLE- MIST ELIMINATOR 3201 702292
GC/MS
SEMI-VOLATILE ANALYSIS
A-13
COMPOUND NAME
AMOUNT
DET. LIMIT
N-Nitrosodimethylamine
Phenol
bis(-2-Ghloroethyl>Ether
2-ChloPoohenol
1.3-Dichlorobenzene
1.4-Dichlorobenzene
1.2-Dichlorobenzene
bis(2-chloroisoprppyl)Ether
N-Nitrpso-Di-Propylamine
Hexachloroethane
Nit robenzene
Isophorone
2-Ni t ropheno1
2.4-Dime thyIpheno1
bis(-2-Chlproethoxy)Me thane
2.4-Dichlorophenol
1.2,4-Trichlorobenzene
Naphtha lene
Hexachlorobutadiene
4-Chloro-3-Methylphenol
Hexachlorocyclopentadiene
2 ,4,6-Trichlorophenol
2-Chloronaohthalene
Dimethyl Phthalate
Acenaohthylene
2 ,6-Dinitrotoluene
Acenaphthene
2,4-Dinitrpphenpl
4-Nit rophenp1
2.4-Dinitrptpluene
Diethylphthalate
4-Chlorppheny1-phenylather
Fluprene
Benzidine
4,6-Dinitrp-2-MethyIphenp1
N-Nitrpsodiphenylamina
4-Brpmppheny1-phenylether
Hexachlorpbenzene
Pentachloropheno1
Phenanthrene
Anthracene
Di-N-Butylphthalate
F lupranthene
ND
NO
ND
ND
ND
ND
ND
ND
ND
ND
53.
ND
ND
140.
ND
ND
ND
60.
ND
55.
ND
ND
ND
ND
50.
ND
71.
420.
ND
ND
ND
ND
ND
ND
530.
310.
ND
ND
ND
620.
170.
ND
220.
40
40
40
40
40
40
40
40
40
40
40
40
40
40
40
40
40
40
40
40
40
40
40
40
40
40
40
200
40
40
40
40
40
40
200
40
40
40
200
40
40
40
40
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
UQ/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
UQ/L
CanoideEnvircnmentsl
-------
A-14
MCKIN
702292
PAGE 2
LP-1840
Pyrene
Butylbenzylohthalate
3.3'-Dichlorobenzidine
Benzo(a)Anthracene
bis-(2-Ethylhexyl)Phthalate
Chrysene
Di-N-Octyl Phthalate
Benzo(b)Fluoranthene
Benzo(k)Fluoranthene
Benzo(a)Pyrene
Indenod .2.3-cd)Pyrene
Oibenzo(a.n)Anthracene
Benzo(Q ,h,i)Pervlene
71.
ND
NO
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
40
40
60
40
40
40
40
40
40
40
40
40
40
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ua/L
Anal vat
Checked Bv
CanonleEnvircnmenlal
-------
Client ID: MCKIN
Sample ID: 64-130-1966
Matrix : WATER
Data File:>64066
SAMPLE- SCRUBBER LIQUID 704066
GC/MS
SEMI-VOLATILE ANALYSIS
A-15
COMPOUND NAME
AMOUNT
N-NitPosod imethylamine
Phenol
bis(-2-ChloPoethyl)Ether
2-Ch1oropheno1
1 ,3-Dich lop.obenzene
1,4-Dichlopobenzene
1,2-DichloPobenzene
bis(2-chloroisopropyl)Ether
N-Nitroso-Di-Propylemine
Hexachloroethane
Ni t robenzene
Isophorone
2-Nitpopheno1
2,4-Dimethylphenol
bis(-2-ChloPoethoxy)Methane
2,4-Dichlopophenol
1,2,4-TrichloPobenzene
Naph'thalene
Hexachlorobutadiene
4-Chlopo-3-Methylphenol
Hexachlorocyclopentadiene
2,4,6-Trichlorophenol
2-Chloronaphthalene
Dimethyl Phthalate
Acenaphthylene
2,6-Dinitrotoluene
Acenaphthene
2,4-Dinitropheno1
4-Ni t ropheno1
2,4-Dinitrotoluene
Diethylphthalate
4-Chlopophenyl-phenylether
Fluopene
Benzidine
4,6-DinitPO-2-Methylphenol
N-Ni t posodipheny1amine
4-Bpomophenyl-phenylethep
Hexachlopobenzene
Pen t achlopopheno1
Phenanthpene
Anthracene
Di-N-Butylphthalate
Fluoranthene
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
57.
ND
ND
64.
ND
ND
ND
ND
ND
ND
92.
ND
ND
32.
DET. LIMIT
30 ug/L
30 ug/L
30 ug/L
30 ug'L
30 ug/L
30 ug/L
30 ug/L
30 ug/L
30 ug/L
30 ug/L
30 ug/L
30 ug/L
30 ug/L
30 ug/L
30 ug/L
30 ug/L
30 ug/L
30 ug/L
30 ug/L
30 ug/L
30 ug/L
30 ug/L
30 ug/L
30 ug/L
30 ug/L
30 ug/L
30 ug/L
150 ug/L
30 ug/L
30 ug/L
30 ug/L
30 ug/L
30 ug/L
30 ug/L
150 ug/L
30 ug/L
30 ug/L
30 ug/L
150 ug/L
30 ug/L
30 ug/L
30 ug/L
30 ug/L
CanonieEnvironmentai
-------
A-16
nCKIN
704066 LP-1986
PAGE 2
Pyrene 54. 30 ug/L
ButyIbenzyIphthalate NO 30 ug/L
3,3'-Dichlopobenzidine NO 60 ug/L
Benzo(a)Anthracene NO 30 ug/L
bis-<2-Ethylhexyl>Phthalate NO 30 ug/L
Chrysene ND 30 ug/L
Di-N-Octyl Phthalate ND 30 ug/L
Benzo(b)Fluoranthene ND 30 ug/L
Benzo(k)Fluoranthene ND 30 ug/L
Benzo(a)Pyrene ND 30 ug/L
Indenod ,2,3-cd)Pyrene ND 30 ug/L
Dibenzo(a,h)Anthracene ND 30 ug/L
Benzo(g,h , i )Perylene ND 30 ug/L
Analyst Checked By
-------
A-17
Cli.nt 1D:MCK1N
S«mpl« 10:84-130-1986
Matrix : WATER
Data File: >X4066
SAMPLE:SCRUBBER LIQUID 704066
GC/MS
VOLATILE ANALYSIS
COMPOUND NAME
DICHLORODIFLUOROMETHANE
CHLOROMETHANE
BROMOMETHANE
VINYL CHLORIDE
CHLOROETHANE
METHYLENE CHLORIDE
TRICHLOROFLUOROMETHANE
1,1-DICHLOROETHENE
1,1-DICHLOROETHANE
TOTAL 1,2-DICHLOROETHENE
CHLOROFORM
1,2-DICHLOROETHANE
1,1,1-TRICHLOROETHANE
CARBON TETRACHLORIDE
BROMODICHLOROMETHANE
1,2-DICHLOROPROPANE
TRANS-1,3-DICHLOROPROPENE
TRICHLOROETHENE
BENZENE
DIBROMOCHLOROMETHANE
1,1,2-TRICHLOROETHANE
CIS-1,3-0ICHLOROPROPENE
2-CHLOROETHYL VINYL ETHER
BROMOFORM
1,1,2,2-TETRACHLOROETHANE
TETRACHLOROETHENE
TOLUENE
CHLOROBENZENE
ETHYL BENZENE
1,3-DICHLOROBENZENE
1,2-DICHLOROBENZENE
1,4-DICHLOROBENZENE
SURROGATE STANDARD
D4-1,2-DICHLOROETHANE (SURR)
D8-TOLUENE (SURR)
4-BROMOFLUOROBENZENE (SURR)
AMOUNT
ND
ND
ND
ND
ND
91.
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
51.
ND
ND
ND
81.
ND
ND
ND
ND
ND
ND
ND
DET. LIMIT
XRECOUEf
101.0
107.4
70.2
50.0
100.0
100.0
100.0
100.0
50.0
50.0
50.0
50.0
50.0
50.0
50.0
50.0
50.0
50.0
50.0
50.0
50.0
50.0
50.0
50.0
50.0
100.0
50.0
50.0
50.0
50.0
50.0
50.0
50.0
50.0
50.0
?Y
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
-------
Table j
Results of PCB's Analysis on Soil
Samples Received From Fairchild, McKin
Results in mg/kg
10-Ui-mb
84-130-1264
Page 3
Sampler ID:
Lab 101:
Analyte(s)
PCB's quantified as PCB 1242
PCB's quantified as PCB 1254
PCB's quantified as PCB 1260
Fuel Tank
Compos i te
612268-9
NO 0.1
NO 0.1
NO 0.1
Analyst
Note:
NO X denotes none detected to d level of X.
TYMI mem fa 1
CD
-------
APPENDIX B
EXCAVATION, SAMPLING AND ANALYTICAL VERIFICATION -
PETROLEUM AREAS l(a,c) AND 2
CanonieEnvironrr
-------
CanonieEnvironmental
B-l
Canonie Environmental Sendees Corj
800 Canonie Drive
Poner. Indiana 46304
Phone 2194264651
March 16, 1987
CH 84-130
Mr. Steven Serlan
Superfund Branch
Waste Management Division
U.S. Environmental Protection Agency
JFK Federal Building HEM-1907
Boston, MA 02203
EXCAVATION. SAMPLING AND ANALYTICAL VERIFICATION
PETROLEUM AREAS l(a.c) AND 2
McKIN SUPERFUND SITE
GRAY. MAINE
Dear Mr. Serlan:
Canonie Environmental Services Corp. (Canonie), In accordance with U.S.
EPA's letter to Canonie of November 26, 1986, has excavated the site
petroleum areas l(a,c) and 2, separated the oily soils from the oily de-
bris, securely stockpiled the separated Items, and sampled and analyzed
the extent of excavation 1n each area. The excavation was completed on
December 12, 1986. The following describes an explanation of the ex-
cavation, sampling and analytical results of each area.
AREA 1 EXCAVATION
The oily soils located In area 1 were excavated by a backhoe using vis-
ual Inspection in determining the lateral and vertical limits of excava-
tion. To verify the visual Inspection, a sampling and laboratory an-
alytical protocol, approved by USEPA and MOEP, was Implemented. Six
samples were taken to verify the lateral excavation perimeter and six
samples were taken to confirm the vertical excavation perimeter. The
samples taken for verification of the vertical perimeter were based on a
20-foot by 20-foot grid pattern. The sample locations are denoted on the
enclosed figure.
-------
B-2
Mr. Steven Serian 2 March 16, 1987
The average depth of excavation in area 1 1s approximately 11.5 feet. Ap-
proximately 900 bulk cubic yards of oily soils and 150 bulk cubic yards of
oily debris were' excavated from area l(a,c). The debris was segregated
from the oily soils by a screening process, with the separated materials
securely stockpiled in a manner approved by USEPA and MDEP. The stockpiles
have been secured with an Impermeable cover placed over the stockpiles and
a sand berm placed around the foot of the stockpiles will prevent any pos-
sible leaching of constituents.
The analytical results from the verification samples taken are enclosed in
this transmlttal. Lateral verification samples were analyzed for add/
base/neutral extractable organics (EPA method 8270), volatile and aromatic
organlcs (EPA method 8010/8020), PCB's, total extractable hydrocarbons, and
EP Toxic Metals. Vertical verification samples were analyzed for EPA method
8270, EPA method 8010/8020, total extractable hydrocarbons, and 10X for
PCB's and 20X for EP Toxic Metals.
Sampling point Al-9 analysis resulted in a xylene concentration of 4.1 mg/
kg and an ethylbenzene concentration of 0.7 mg/kg. Canonie excavated ad-
ditional yardage around this sampling location because of the xylene con-
centration. A ten-foot radial excavation was centered on sampling point
Al-9, five-feet deep resulting in approximately 60 cubic yards of soil. Ad-
ditional samples were taken to verify this excavation, Al-15 and Al-17 on
the north and south sides, and Al-16 on the bottom of the new excavation.
Al-15 and Al-17 were analyzed for 8010/8020 and resulted in non-detectable
concentrations. Al-16 was analyzed for 8010/8020, 8270, and TEH. Al-16 an-
alysis resulted in non-detectable concentrations, and TEH resulted in a con-
centration of 8 mg/kg.
Sampling point Al-2 revealed a number of polycycllc aromatic hydrocarbons,
with three PAH's detected at or above 1 mg/kg. Because of these concentra-
tions, Canonie excavated additional yardage around this sampling point. An
area was excavated that extended ten-feet east and west of this side slope
sampling point, and 7.5 feet south. The depth of this additional excava-
tion was eleven-feet, resulting in a total of 60 cubic yards of soil. Two
additional samples were taken to verify the excavation; Al-13 was taken on
the newly excavated south side, and Al-14 was taken on the newly excavated
bottom. The two samples were composited in Canonie1s Stockton, CA labor-
atory for PAH analysis. The composite analysis resulted in non-detectable
PAH concentrations at 0.33 mg/kg.
Side slope verification sampling point Al-12 resulted in a number of pos-
itive PAH concentrations, with one analyte corresponding to a concentration
greater than 1 mg/kg. However, these soils have already been excavated and
aerated with "solvent" area l(b) soils.
Test pits were dug through and 20 feet adjacent to each side of the origin-
al borehole sampling Vocations 1-31, 1-32, and 1-33, and extended 13 feet
CaitOItleEnvironmental
-------
B-3
Mr. Steven Serian 3 March 16, 1987
deep. Very small pockets of visually discolored oily material, at a depth
of approximately.11 feet were removed and stockpiled, amounting to approx-
imately 10 cubic yards of material. It was observed that this thin line of
oily-looking material represents the original ground surface, before 10
feet of fill material was placed over the original ground surface. This
black, loamy layer is comprised of the original vegetation which had de-
cayed when fill material was placed above. An abundance of plant and tree
root systems unearthed at this depth supports this conclusion.
Samples were then taken at a depth of 11 feet. Samples Al-18, Al-19, and
Al-20 were taken in the same location as original borehole sampling points
1-33, 1-32, and 1-31 respectively. Samples Al-18-20 were analyzed for
8010/8020, 8270, TEH, EP Toxic Metals, and PCB's. The only significant
detectable analytical result was a positive TEH concentration at sampling
location Al-18. As noted previously, the positive result 1s due to the
natural organic fraction of the decayed vegetation. This statement can
be justified based on the absence of volatile and aromatic organlcs and
polycyclic aromatic compounds, which existed in the oily soils associated
with off-site originated petroleum components. Therefore, Canonie proposes
no additional action for the soils surrounding sampling location Al-18.
AREA 2 EXCAVATION
The oily soils located in area 2 were excavated by a backhoe using the same
parameters 1n determining the limits of excavation as soils 1n area 1. The
same sampling and laboratory analytical program described to verify the lat-
eral and vertical extent of excavation in area 1 was used in area 2. Five
samples were taken to verify the vertical excavation perimeter, three samples
were taken to verify the lateral excavation perimeter, and one sample was
taken to represent both the lateral and vertical excavation perimeter. Sam-
ple locations are denoted on the enclosed figure.
The depth of excavation was approximately 10.5 feet, with the exception of
two ramped areas. One ramped area lies adjacent and perpendicular to the
horizontal alignment of soil borings 2-7 and 2-14. The area west of this
alignment slopes upward to the west until it reaches natural ground surface.
The other ramped area 1s adjacent and north of the east-west alignment of
soil borings 2-7 and 2-9. The area begins ten-feet to the east of soil
boring 2-8 and continues ten-feet west of that location. This ramped area
also slopes upward until the natural ground surface 1s encountered.
Approximately 800 cubic yards of oily soils and approximately 150 cubic
yards of oily covered-debris were excavated from area 2. The sample depths
and laboratory analytical results are presented 1n the appropriate tables.
Samples A2-2, A2-4, A2-5, and A2-7 were not analyzed for TEH. The samples
CanontoEnvironmentdl
-------
B-4
Mr. Steven Serlan 4 March 16, 1987
were analyzed for EPA method 8270, 8010/8020, PCB's and EP Toxic Metals.
The sample mass was not sufficient to perform all the analyses, and the
choice between analysis of 8270 and TEH needed to be assessed. Canonie
regarded the 8270 analysis as more Indicative of the presence of priority
pollutants. Therefore 8270 was performed In Heu of testing for TEH for
these samples. Area 2 was backfilled before this Issue needed to be ad-
dressed. Additionally, A2-1 was not analyzed at all because 1t was Inad-
vertently lost to the routine "house-cleaning" of samples. This pro-
cedure Involves the discarding of samples held for a duration greater
than the alotted two weeks. Sample A2-1 was mistaken for another sample,
and was discarded.
After review of the analytical results, Canonie asserts that the missing
analyses reported previously do not Impact the final Interpretation of the
data. It 1s clear that all petroleum substances have been removed, from
review of 8010/8020 and 8270 analytical results.
Canonie has performed this sampling and analytical protocol in compliance
with USEPA and MOEP's excavation verification criteria. Canonie certifies
that the results of these procedures indicate that all petroleum originated
substances from an off-site origin have been completey removed.
Canonie trusts this presentation of the sampling protocol followed by the
support of analytical results verifies the complete removal of petroleum
substances which existed 1n site areas l(a,c) and 2. If you have any
questions or comments, please call.
Very truly yours,
Brian M. Bell
Project Engineer
Operations Coordinator
McKin Superfund Site
Enclosure
BMB/ts
cc: John Kuruc, Amoco Corporation
E. F. Skoczen, Canonie Environmental Services Corp.
Central File, Canonie Environmental Services Corp.
Deborah Schmall, Landels, Rlpley & Diamond
Rebecca Hewett, Maine Department of Environmental Protection
CanontoEnvironmental
-------
C-31
Table 2. Semivolatile Organic Results
Canonie Sample ID
8270 Compounds
Phenol
Bis (2-chloroethyl) ether
2-Chlorophenol
1,3-Dichlorobenzene
1,4-Dichlorobenzene
1 ,2-Dichlorobenzene
B is (2-chloroisopropyl) ether
N-Nitroso-di-n-propylamine
Hexachloroethane
Nitrobenzene
Isophorone
2-Nitrophenol
2,4-Dimethylphenol
Bis(2-chloroethoxy)methane
2,4-Dichlorophenol
1 ,2,4-Trichlorobenzene
Naphthalene
Hexachlorobutadiene
4-Chloro-3-methyl phenol
Hexachlorocyclopentadiene
2,4,6-Trichlorophenol
2-Chloronaphthalene
Dimethyl phthalate
Acenaphthylene
Acenaphthene
2,4-Dinitrophenol
4-Nitrophenol
2,4-Dinitrotoluene
2,6-Dinitrotoluene
Diethyl phthalate
4-Chlorophenyl-phenyl ether
Fluorene
4 ,6-Dinitro-2-methylphenol
N-Nitrosodiphenylamine
4-Bromophenyl-phenyl ether
Hexachlorobenzene
Pentachlorophenol
Phenanthrene
Anthracene
Oi-n-Butyl phthalate
4-2-16
3470
ug/kg
<330
<330
<330
<330
<330
<660
<330
<1300
<660
<990
<660
<1300
<990
<660
<990
<330
<330
<660
<330
<6600
<660
<330
<330
<330
<330
<6600
<2600
<660
<990
<330
<330
<330
<2000
<1300
<330
<990
<330
1300
630
<660
dupl
4-13-15
3329
ug/kg
<660
<660
<660
<660
<660
<1300
<660
<2600
<1300
<2000
<1300
<2600
<2000
<1300
<2000
<660
<660
<1300
<660
<13000
<1300
<660
<660
<660
<660
<13000
<5300
<1300
<2000
<660
<660
<660
<4000
<2600
<660
<2000
<660
1800
<660
<1300
method
blank
ug/kg
<33
<33
<33
<33
<33
<66
<33
<130
<66
<99
<66
<130
<99
<66
<99
<33
<33
<66
<33
<660
<66
<33
<33
<33
<33
<660
<260
<66
<99
<33
<33
<33
<200
<130
<33
<99
<33
<33
<33
<66
Canonie
8704041
Page 6 of
-------
C-32
Canonie
8704041
Page 7 of 7
Table 2. Semi volatile Organic Results (continued)
Canonie Sample ID
8270 Compounds
Fluoranthene
Pyrene
Butyl benzyl phthalate
3,3-Dichlorobenzidine
Benzo (a) anthracene
Bis (2-ethylhexyl) phthalate
Chrysene
Di-n-octyl phthalate
Benzo (b)fluoranthene
Benzo(k)fluoranthene
Benzo(a)pyrene
Indeno(l,2,3-cd)pyrene
Oibenzo( a, h) anthracene
Benzo (g,h,i)perylene
Alpha-BHC
Beta-BHC
Gamma-BHC
Delta-BHC
Heptachlor
Aldrin
Heptachlor epoxide
Endosulfan I
Dieldrin
4,4'-DDE
Endrin
Endosulfan II
4,4'-DDD
Endrin aldehyde
Endosulfan sulfate
4, 4 '-DDT
PCB's
Surrogates
2-Fluorophenol
Phenol-d5
Nitrobenzene-d5
2-Fluorobiphenyl
2,4,6-Tribromophenol
p-Terphenyl-d!4
4-2-16
3470
ug/kg
<990
<660
<990
<6600
<330
<660
<330
<660
<1300
<1300
<330
<330
<990
<660
<3300
<3300
<3300
<3300
<3300
<3300
<3300
<3300
<3300
<3300
<3300
<3300
<3300
<3300
<3300
<3300
<3300
dupl
4-13-15
3329
ug/kg
<2000
<1300
<2000
<13000
<660
<1300
<660
<1300
<2600
<2600
<660
<660
<2000
<1300
<6600
<8600
<6600
<6600
<6600
<6600
<6600
<6600
<6600
<6600
<6600
<6600
<6600
<6600
<6600
<6600
<6600
method
blank
ug/kg
<99
<66
<99
<660
<33
<66
<33
<66
<130
<130
<33
<33
<99
<66
<330
<330
<330
<330
<330
<330
<330
<330
<330
<330
<330
<330
<330
<330
<330
<330
<330
Percent Recovery (X)
59
62
32
78
0
46
69
62
40
82
@
68
86
75
80
92
63
81
- surrogate diluted below detection limit
-------
C-33
Canonie
8704015
Page 4 of 5
Table 2. Semivolatile Organic Results
Canonie Sample ID
8270 Compounds
4-3-6 4-3-13
ug/kg ug/kg
Phenol <330 <330
bis(2-Chloroethyl)Ether <330 <330
2-Chlorophenol <330 <330
1,3-Dichlorobenzene <330 <330
1,4-Oichlorobenzene <330 <330
1,2-Dichlorobenzene <660 <660
bis(2-Chloroisopropyl)Ether <330 <330
N-Nitroso-Di-n-Propylamine <1300 <1300
Hexachloroethane <660 <660
Nitrobenzene <990 <990
Isophorone <660 <660
2-Nitrophenol <1300 <1300
2,4-Dimethylphenol <990 <990
bis(2-Chloroethoxy)Methane <660 <660
2,4-Oichlorophenol <990 <990
1,2,4-Trichlorobenzene <330 <330
Naphthalene <330 <330
Hexachlorobutadiene <660 <660
4-Chloro-3-Methylphenol <330 <330
Hexachlorocyclopentadiene <6600 <6500
2,4,6-Trichlorophenol <660 <660
2-Chloronaphthalene <330 <330
Dimethyl Phthalate <330 <330
Acenaphthylene <330 <330
Acenaphthene <330 <330
2,4-Dinitrophenol <6600 <6600
4-Nitrophenol <2600 <2600
2,4-Dinitrotoluene <660 <660
2,6-Dinitrotoluene <990 <990
Diethylphthalate <330 <330
4-Chlorophenyl-Phenylether <330 <330
Fluorene <330 <330
4,6-D1nitro-2-Hethylphenol <2000 <2000
N-Nitrosodiphenylam1ne <1300 <1300
4-Bromophenyl-Phenylether <330 <330
Hexachlorobenzene <990 <990
Pentachlorophenol <330 <330
Phenanthrene 830 790
Anthracene <330 430
Di-n-Butylphthalate <660 <660
-------
C-3<
Canonie
8704015
Page 5 of 5
Table 2. Semivolatile Organic Results (continued)
Canonie Sample ID
8270 Compounds
Fluoranthene
Pyrene
Butylbenzylphthalate
3,3-Dichlorobenzidine
8enzo(a)Anthracene
bis(2-Ethylhexyl)Phthalate
Chrysene
Di-n-Octyl Phthalate
Ben zo(b) Fluoranthene
Benzo( k) Fl uoranthene
Ben zo( a) Pyrene
Indeno(l, 2, 3-cd) Pyrene
Dibenzo(a.h) Anthracene
Benzo(g,h,i)Perylene
Alpha-BHC
Beta-BHC
Gamma -BHC
Oelta-BHC
Heptachlor
Aldrin
Heptachlor Epoxide
Endosulfan I
Dieldrin
4,4'-DDE
Endrin
Endosulfan II
4,4'-DDD
Endrin Aldehyde
Endosulfan Sulfate
4,4'-DDT
PCB's
4-3-6
ug/kg
<990
<660
<990
<6600
<330
<660
<330
<660
<1300
<1300
<330
<330
<990
<660
<3300
<3300
<3300
<3300
<3300
<3300
<3300
<3300
<3300
<3300
<3300
<3300
<3300
<3300
<3300
<3300
<3300
4-3-13
ug/kg
<990
<660
<990
<6600
<330
<660
<330
<660
<1300
<1300
<330
<330
<990
<660
<3300
<3300
<3300
<3300
<3300
<3300
<3300
<3300
<3300
<3300
<3300
<3300
<3300
<3300
<3300
<3300
<3300
Surrogates
Percent Recovery (I)
2-Fluoro phenol
Phenol-d5
Nitrobenzene-d5
2-Fluorobiphenyl
2,4, 6-Tr ibromophenol
p-Terphenyl-d!4
49
54
40
60
90
68
53
57
67
74
32
52
-------
C-35
Canonie
8704026
Page 4 of
Table 2. Semivolatile Organic Results
Canonie Sample ID
8270 Compounds
4-7-8
ug/kg
Phenol <330
bis(2-Chloroethyl)Ether <330
2-Chlorophenol <330
1,3-Dichlorobenzene <330
1,4-Oichlorobenzene <330
1,2-Oichlorobenzene <660
bis(2-Chloroisopropyl)Ether <330
N-Nitroso-Di-n-Propylamine <1300
Hexachloroethane <660
Nitrobenzene <990
Isophorone <660
2-Nitrophenol <1300
2,4-Dimethylphenol <990
bis(2-Ch1oroethoxy)Methane <660
2,4-Dichlorophenol <990
1,2,4-Trichlorobenzene <330
Naphthalene <330
Hexachlorobutadiene <660
4-Chloro-3-Methylphenol <330
Hexachlorocyclopentadiene <6600
2,4,6-Trichlorophenol <660
2-Chloronaphthalene <330
Dimethyl Phthalate <330
Acenaphthylene <330
Acenaphthene <330
2,4-Dinitrophenol <6600
4-Nitrophenol <2600
2,4-Dinitrotoluene <660
2,6-Dinitrotoluene <990
Diethylphthalate <330
4-Chlorophenyl-Phenylether <330
Fluorene <330
4,6-Din1tro-2-Methylphenol <2000
N-Nitrosod1phenylam1ne <1300
4-Bromophenyl-Phenylether <330
Hexachlorobenzene <990
Pentachlorophenol <330
Phenanthrene 830
Anthracene 500
Di-n-Butylphthalate <660
-------
C-36
Canonie
8704026
Page 5 of 5
8270 Compounds
Table 2. Semivolatile Organic Results (continued)
Canonie Sample ID
4-7-8
ug/kg
Fluoranthene <990
Pyrene <660
Butylbenzylphthalate <990
3,3-Dichlorobenzidine <6600
Benzo(a)Anthracene <330
bis(2-Ethylhexyl)Phtha1ate <660
Chrysene <330
Di-n-Octyl Phthalate <660
Benzo(b)Fluoranthene <1300
Benzo(k)Fluoranthene <1300
Benzo(a)Pyrene <330
Indeno(l,2,3-cd)Pyrene <330
Dibenzo(a.h)Anthracene <990
Benzo(g,h,i)Perylene <660
Alpha-BHC <3300
Beta-BHC <3300
Gamma-BHC <3300
Delta-BHC <3300
Heptachlor <3300
Aldrin <3300
Heptachlor Epoxide <3300
Endosulfan I <3300
Dieldrin <3300
4,4'-DDE <3300
Endrin <3300
Endosulfan II <3300
4,4'-ODD <3300
Endrin Aldehyde <3300
Endosulfan Sulfate <3300
4,4'-DDT <3300
PCB's <3300
Surrogates
2-Fluorophenol
Phenol-d5
Nitrobenzene-d5
2-Fluorobiphenyl
2,4,6-Tr ibromophenol
p-Terphenyl-d!4
Percent Recovery (I)
72
73
59
86
75
98
-------
C-37
Canonie
8704028
Page 4 of 5
Table 2. Semivolatile Organic Results
Canonie Sample ID
4-8-7
4-8-9
8270 Compounds
ug/kg ug/kg
Phenol <330 <330
bis(2-Chloroethyl)Ether <330 <330
2-Chlorophenol <330 <330
1,3-Dichlorobenzene <330 <330
1,4-Dichlorobenzene <330 <330
1,2-Dichlorobenzene <660 <660
bis(2-Chloroisopropyl)Ether <330 <330
N-Nitroso-Di-n-Propylamine <1300 <1300
Hexachloroethane <660 <660
Nitrobenzene <990 <990
4sophorone <660 <660
2-Nitrophenol <1300 <1300
2,4-Dimethylphenol <990 <990
bis(2-Chloroethoxy)Methane <660 <660
2,4-Dichlorophenol <990 <990
1,2,4-Trichlorobenzene <330 <330
Naphthalene <330 <330
Hexachlorobutadiene <660 <660
4-Chloro-3-Hethylphenol <330 <330
Hexachlorocyclopentadiene <6600 <6600
2,4,6-Trichlorophenol <660 <660
2-Chloronaphthalene <330 <330
Dimethyl Phthalate <330 <330
Acenaphthylene <330 <330
Acenaphthene <330 <330
2,4-Dinitrophenol <6600 <6600
4-Nitrophenol <2600 <2600
2,4-Oinitrotoluene <660 <660
2,6-Din1trotoluene <990 <990
Diethylphthalate <330 <330
4-Chlorophenyl-Phenylether <330 <330
Fluorene <330 <330
4,6-Dinitro-2-Hethylphenol <2000 <2000
N-Nitrosodiphenylamine <1300 <1300
4-Bromophenyl-Phenylether <330 <330
Hexachlorobenzene <990 <990
Pentachlorophenol <330 <330
Phenanthrene 660 1700
Anthracene <330 660
Oi-n-Butylphthalate <660 <660
-------
C-38
Canonie
8704028
Page 5 of 5
Table 2. Semivolatile Organic Results (continued)
Canonie Sample ID
8270 Compounds
Fluoranthene
Pyrene
Butyl benzyl phthalate
3,3-Dichlorobenzidine
Benzo(a)Anthracene
bis(2-Ethylhexyl) Phthalate
Chrysene
Di-n-Octyl Phthalate
Benzo( b) Fl uoranthene
Benzo ( k) Fl uoranthene
Ben zo( a) Pyrene
Indeno(l, 2, 3-cd) Pyrene
Dibenzo(a,h)Anthracene
Benzo(g,h,i)Perylene
Alpha-BHC
Beta-BHC
Gamma-BHC
Delta-BHC
Heptachlor
Aldrin
Heptachlor Epoxide
Endosulfan I
Dieldrin
4,4'-DDE
Endrin
Endosulfan II
4,4'-DDD
Endrin Aldehyde
Endosulfan Sulfate
4,4'-DDT
PCB's
4-8-7
ug/kg
<990
<660
<990
<6600
<330
<660
<330
<660
<1300
<1300
<330
<330
<990
<660
<3300
<3300
<3300
<3300
<3300
<3300
<3300
<3300
<3300
<3300
<3300
<3300
<3300
<3300
<3300
<3300
<3300
4-8-9
ug/kg
<990
<660
<990
<6600
<330
<660
<330
<660
<1300
<1300
<330
<330
<990
<660
<3300
<3300
<3300
<3300
<3300
<3300
<3300
<3300
<3300
<3300
<3300
<3300
<3300
<3300
<3300
<3300
<3300
Surrogates
Percent Recovery (%)
2-Fluorophenol
Phenol-d5
Nitrobenzene-d5
2-Fluorobiphenyl
2,4, 6-Tr ibromophenol
p-Terphenyl-d!4
39
46
@
66
9
58
70
73
54
92
@
74
- surrogate diluted below its detection limit
-------
C-3!
Canonie
8704032
Page 2 of 3
. Table 2. Semivolatile Organic Results
Canonie Sample ID
8270 Compounds
4-9-4 4-9-13
ug/kg ug/kg
Phenol <330 <330
bis(2-Chloroethyl)Ether <330 <330
2-Chlorophenol <330 <330
1,3-Dichlorobenzene <330 <330
1,4-Oichlorobenzene <330 <330
1,2-Dichlorobenzene <660 <660
bis(2-Chloroisopropyl)Ether <330 <330
N-Nitroso-Di-n-Propylamine <1300 <1300
Hexachloroethane <660 <660
Nitrobenzene <990 <990
Isophorone <660 <660
2-Nitrophenol <1300 <1300
2,4-Dimethylphenol <990 <990
bis(2-Chloroethoxy)Methane <660 <660
2,4-Dichlorophenol <990 <990
1,2,4-Trichlorobenzene <330 <330
Naphthalene <330 <330
Hexachlorobutadiene <660 <660
4-Ch1oro-3-Methylphenol <330 <330
Hexachlorocyclopentadiene <6600 <6600
2,4,6-Tricnlorophenol <660 <660
2-Chloronaphthalene <330 <330
Dimethyl Phthalate <330 <330
Acenaphthylene <330 <330
Acenaphthene <330 <330
2,4-Oinitrophenol <6600 <6600
4-Nitrophenol <2600 <2600
2,4-Oinitrotoluene <660 <560
2,6-Oin1trotoluene <990 <990
Diethylphthalate <330 <330
4-Chlorophenyl-Phenylether <330 <330
Fluorene <330 <330
4,6-Dinitro-2-Methylphenol <2000 <2000
N-Nitrosodiphenylam1ne <1300 <1300
4-Bromophenyl-Phenylether <330 <330
Hexachlorobenzene <990 <990
Pentachlorophenol <330 <330
Phenanthrene 1500 1800
Anthracene <330 <330
Di-n-Butylphthalate <660 <660
-------
C-40
Canonie
8704032
Page 3 of 3
Table 2. Semivolatile Organic Results (continued)
Canonie Sample ID
8270 Compounds
Fluoranthene
Pyrene
Butyl benzylphthalate
3,3-Dichlorobenzidine
Benzo(a)Anthracene
bis(2-Ethylhexyl)Phtha1ate
Chrysene
Di-n-Octyl Phthalate
Benzo(b) Fluoranthene
Benzo(k)Fluoranthene
Benzo(a)Pyrene
Indeno(l, 2, 3-cd) Pyrene
Oibenzo( a, h) Anthracene
Benzo(g,h,i)Perylene
Alpha-BHC
Beta-BHC
Ganuna-BHC
Delta-BHC
Heptachlor
Aldrin
Heptachlor Epoxide
Endosulfan I
Dieldrin
4, 4 '-ODE
Endrin
Endosulfan II
4,4'-ODD
Endrin Aldehyde
Endosulfan Sulfate
4, 4 '-DDT
PCB's
Surrogates
2-Fluorophenol
Phenol -d5
Nitrobenzene-d5
2-Fluorobiphenyl
2 ,4 ,6-Tri bromophenol
p-Terphenyl-d!4
4-9-4
ug/kg
<990
690
<990
<6600
<330
<660
<330
<660
<1300
<1300
<330
<330
<990
<660
<3300
<3300
<3300
<3300
<3300
<3300
<3300
<3300
<3300
<3300
<3300
<3300
<3300
<3300
<3300
<3300
<3300
Percent
9
9
9
9
8
9
4-9-13
ug/kg
<990
830
<990
<6600
<330
<660
<330
<660
<1300
<1300
<330
<330
<990
<660
<3300
<3300
<3300
<3300
<3300
<3300
<3300
<3300
<3300
<3300
<3300
<3300
<3300
<3300
<3300
<3300
<3300
Recovery (%)
9
9
9
9
9
9
9 - surrogates diluted out
-------
C-41
Canonie
8704036
Page 4 of
Table 2. Semi volatile Organic Results
Canomie Sample ID
8270 Compounds
Phenol
bis(2-Chloroethyl)Ether
2-Chlorophenol
1,3-Dichlorobenzene
1 ,4-Dichlorobenzene
1 ,2-Oichlorobenzene
bis(2-Chloroisopropyl)Ether
N-Nitroso-Di-n-Propylamine
Hexachloroethane
Nitrobenzene
Isophorone
2-Nitrophenol
2,4-Dimethylphenol
bis(2-Chloroethoxy) Methane
2,4-Oichlorophenol
1,2,4-Trichlorobenzene
Naphthalene
Hexachlorobutadiene
4-Chloro-3-Methyl phenol
Hexach 1 orocycl opentad i ene
2,4,6-Trichlorophenol
2-Chloronaphthalene
Dimethyl Phthalate
Acenaphthylene
Acenaphthene
2,4-Dinitrophenol
4-Nitrophenol
2,4-Dinitrotoluene
2,6-Oinitrotoluene
Diethylphthalate
4-Chlorophenyl-Phenylether
Fluorene
4 ,6-Oinitro-2-Metnylphenol
N-Nitrosodiphenylamine
4-Bromophenyl -Phenylether
Hexachlorobenzene
Pentachlorophenol
Phenanthrene
Anthracene
Di-n-Butylphthalate
4-10-18
3468
ug/kg
<170
<170
<170
<170
<170
<330
<170
<660
<330
<500
<330
<660
<500
<330
<500
<170
<170
<330
<170
<3300
<330
<170
<170
<170
<170
<3300
<1300
<330
<500
<170
<170
<170
<990
<660
<170
<500
<170
810
300
<330
method
blank
ug/kg
<33
<33
<33
<33
<33
<66
<33
<130
<66
<99
<66
<130
<99
<66
<99
<33
<33
<66
<33
<660
<66
<33
<33
<33
<33
<660
<260
<66
<99
<33
<33
<33
<200
<130
<33
<99
<33
<33
<33
<66
-------
C-42
Canonie
8704036
Page 5 of 5
Table 2. Semivolatile Organic Results (continued)
Canomie Sample ID
8270 Compounds
Fluoranthene
Pyrene
Butylbenzylphthalate
3,3-Dichlorobenzidine
Benzo(a) Anthracene
bis(2-Ethylhexyl)Phthalate
Chrysene
Di-n-Octyl Phthalate
Benzo(b) Fluoranthene
Benzo( k) Fluoranthene
8enzo(a)Pyrene
Indeno(l,2,3-cd)Pyrene
D ibenzof a, h) Anthracene
Benzo(g,h,i)Perylene
Alpha-BHC
Beta-BHC
Gamma -BHC
Delta-BHC
Heptachlor
Aldrin
Heptachlor Epoxide
Endosulfan I
Dieldrin
4,4'-ODE
Endrin
Endosulfan II
4, 4 '-ODD
Endrin Aldehyde
Endosulfan Sulfate
4, 4 '-DDT
PCB's
Surrogates
2-Fluorophenol
Phenol -d5
Nitrobenzene-d5
2-Fluorobiphenyl
2,4,6-Tribromophenol
p-Terphenyl-d!4
4-10-18 method
3468 blank
ug/kg ug/kg
<500 <99
450 <66
<500 <99
<3300 <660
<170 <33
<330 <66
<170 <33
<330 <66
<660 <130
<660 <130
<170 <33
<170 <33
<500 <99
<330 <66
<1700 <330
<1700 <330
<1700 <330
<1700 <330
<1700 <330
<1700 <330
<1700 <330
<1700 <330
<1700 <330
<1700 <330
<1700 <330
<1700 <330
<1700 <330
<1700 <330
<1700 <330
<1700 <330
<1700 <330
Percent Recovery (JL)
60 60
55 59
57 68
78 77
8 0
62 82
0 - surrogate diluted below its detection limit
-------
C-43
Canonie
8704041
Page 4 of 7
Table 2. Semivolatile Organic Results
Canonie Sample ID
8270 Compounds
4-2-4 4-2-6 4-2-8 4-13-3 4-13-15
3271 3273 3275 3324 3329
ug/kg ug/kg ug/kg ug/kg ug/kg
Phenol
Bis (2-chloroethyl) ether
2-Chlorophenol
1,3-Dichlorobenzene
1,4-Dichlorobenzene
1,2-Dichlorobenzene
Bis(2-chloroisopropyl) ether
N-Nitroso-di-n-propylamine
Hexachloroethane
Nitrobenzene
Isophorone
2-Nitrophenol
2,4-Dimethylphenol
8is(2-chloroethoxy)methane
2,4-Dichlorophenol
1 ,2,4-Trichlorobenzene
Naphthalene
Hexachlorobutadiene
4-Chloro-3-methyl phenol
Hexachlorocyclopentadiene
2,4,6-Trichlorophenol
2-Chloronaphthalene
Dimethyl phthalate
Acenaphthylene
Acenaphthene
2,4-Dinitrophenol
4-Nitrophenol
2,4-Dinitrotoluene
2,6-Dinitrotoluene
Diethyl phthalate
4-Chlorophenyl-phenyl ether
Fluorene
4,6-Dinitro-2-methylpheno1
N-Nitrosodiphenylamine
4-Bromophenyl-phenyl ether
Hexachlorobenzene
Pentachlorophenol
Phenanthrene
Anthracene
Di-n-Butyl phthalate
<330
<330
<330
<330
<330
<660
<330
<1300
<660
<990
<660
<1300
<990
<660
<990
<330
<330
<660
<330
<6600
<660
<330
<330
<330
<330
<6600
<2600
<660
<990
<330
<330
<330
<2000
<1300
<330
<990
<330
1600
<330
<660
<330
<330
<330
<330
<330
<660
<330
<1300
<660
<990
<660
<1300
<990
<660
<990
<330
<330
<660
<330
<6600
<660
<330
<330
<330
<330
<6600
<2600
<660
<990
<330
<330
<330
<2000
<1300
<330
<990
<330
1300
<330
<660
<330
<330
<330
<330
<330
<660
<330
<1300
<660
<990
<660
<1300
<990
<660
<990
<330
<330
<660
<330
<6600
<660
<330
<330
<330
<330
<6600
<2600
<660
<990
<330
<330
<330
<2000
<1300
<330
<990
<330
1400
<330
<660
<330
<330
<330
<330
<330
<660
<330
<1300
<660
<990
<660
<1300
<990
<660
<990
<330
<330
<660
<330
<6600
<660
<330
<330
<330
<330
<6600
<2600
<660
<990
<330
<330
<330
<2000
<1300
<330
<990
<330
1100
<330
<660
<330
<330
<330
<330
<330
<660
<330
<1300
<660
<990
<660
<1300
<990
<660
<990
<330
<330
<660
<330
<6600
<660
<330
<330
<330
<330
<6600
<2600
<660
<990
<330
<330
<330
<2000
<1300
<330
<990
<330
1100
<330
<660
-------
C-44
Canonie
8704041
Page 5 of 7
Table 2. Semivolatile Organic Results (continued)
Canonie Sample 10
8270 Compounds
Fluoranthene
Pyrene
Butyl benzyl phthalate
3,3-Dichlorobenzidine
Senzo(a) anthracene
Bis(2-ethylhexyl)phthalate
Chrysene
Di-n-octyl phthalate
Benzo(b) f luoranthene
Benzo(k)fluoranthene
Benzo(a)pyrene
Indeno(l,2,3-cd)pyrene
0 ibenzo( a, h) anthracene
Benzo(g,h,i)pery1ene
Alpha-BHC
Beta-BHC
Gamma ~8HC
Delta-BHC
Heptachlor
Aldrin
Heptachlor epoxide
Endosulfan I
Dieldrin
4,4'-DOE
Endrin
Endosulfan II
4,4'-OOD
Endrin aldehyde
Endosulfan sulfate
4,4'-DDT
PCB's
Surrogates
2-Fluorophenol
Phenol-d5
Nitrobenzene-d5
2-Fluorobiphenyl
2,4,6-Tribromophenol
p-Terphenyl-d!4
4-2-4
3271
ug/kg
<990
<660
<990
<5600
<330
<660
<330
<660
<1300
<1300
<330
<330
<990
<660
<3300
<3300
<3300
<3300
<3300
<3300
<3300
<3300
<3300
<3300
<3300
<3300
<3300
<3300
<3300
<3300
<3300
Percent
53
55
9
86
0
54
4-2-6
3273
ug/kg
<990
690
<990
<6600
<330
<660
<330
<660
<1300
<1300
<330
<330
<990
<660
<3300
<3300
<3300
<3300
<3300
<3300
<3300
<3300
<3300
<3300
<3300
<3300
<3300
<3300
<3300
<3300
<3300
Recovery (X)
59
59
36
74
9
38
4-2-8
3275
ug/kg
<990
<660
<990
<6600
<330
<660
<330
<660
<1300
<1300
<330
<330
<990
<660
<3300
<3300
<3300
<3300
<3300
<3300
<3300
<3300
<3300
<3300
<3300
<3300
<3300
<3300
<3300
<3300
<3300
62
55
@
62
9
56
4-13-3
3324
ug/kg
<990
<660
<990
<6600
<330
<660
<330
<660
<1300
<1300
<330
<330
<990
<660
<3300
<3300
<3300
<3300
<3300
<3300
<3300
<3300
<3300
<3300
<3300
<3300
<3300
<3300
<3300
<3300
<3300
53
55
30
68
0
48
4-13-15
3329
ug/kg
<990
<660
<990
<6600
<330
<660
<330
<660
<1300
<1300
<330
<330
<990
<660
<3300
<3300
<3300
<3300
<3300
<3300
<3300
<3300
<3300
<3300
<3300
<3300
<3300
<3300
<3300
<3300
<3300
59
59
20
70
9
52
- surrogate diluted below detection limit
-------
C-45
Canonie
3704046
Page 4 of 5
Table 2. Semivolatile Organic Results
Canonie Sample ID
4-14-4 4-14-13
8270 Compounds ug/kg ug/kg
Phenol <170 <170
Bis(2-chloroethyl)ether <170 <170
2-Chlorophenol <170 <170
1,3-Dichlorobenzene <170 <170
1,4-Oichlorobenzene <170 <170
1,2-Dichlorobenzene <330 <330
Bis(2-chloroisopropyl)ether <170 <170
N-M-troso-di-n-propylamine <660 <660
Hexachloroethane <330 <330
Nitrobenzene <500 <500
Isophorone <330 <330
2-Nitrophenol <660 <660
2,4-Dimethylphenol <500 <500
Bis(2-chloroethoxy)methane <330 <330
2,4-Dichlorophenol <500 <500
1,2,4-Trichlorobenzene <170 <170
Naphthalene <170 <170
Hexachlorobutadiene <330 <330
4-Chloro-3-methylphenol <170 <170
Hexachlorocyclopentadiene <3300 <3300
2,4,6-Trichlorophenol <330 <330
2-Chloronaphthalene <170 <170
Dimethyl phthalate <170 <170
Acenaphthylene <170 <170
Acenaphthene <170 <170
2,4-Dinitrophenol <3300 <3300
4-Nitrophenol <1300 <1300
2,4-Dinitrotoluene <330 <330
2,6-Dinitrotoluene <500 <500
Oiethyl phthalate <170 <170
4-Chlorophenyl-phenyl ether <170 <170
Fluorene <170 310
4,6-Dinitro-2-methylphenol <990 <990
N-Nitrosodiphenylamine <660 <660
4-8romophenyl-phenyl ether <170 <170
Hexachlorobenzene <500 <500
Pentachlorophenol <170 <170
Phenanthrene 1500 1700
Anthracene <170 <170
Oi-n-Butyl phthalate <330 <330
-------
C-46
Canonie
8704046
Page 5 of 5
Table 2. Semivolatile Organic Results (continued)
Canonie Sample ID
4-14-4 4-14-13
8270 Compounds
Fluoranthene
Pyrene
Butyl benzyl phthalate
3,3-Dichlorobenzidine
Benzo(a)anthracene
Bis (2-ethylhexyl) phthalate
Chrysene
Di-n-octyl phthalate
Benzo(b)fluoranthene
Benzo(k)fluoranthene
Benzo(a)pyrene
Indeno(l,2,3-cd)pyrene
Dibenzo( a, h) anthracene
Benzo(g,h,i)perylene
Alpha-BHC
Beta-BHC
Gamma -BHC
Delta-BHC
Heptachlor
Aldrin
Heptachlor epoxide
Endosulfan I
Dieldrin
4, 4 '-DDE
Endrin
Endosulfan II
4,4'-DOO
Endrin aldehyde
Endosulfan sulfate
4, 4 '-DDT
PCB's
Surrogates
2-Fluorophenol
Phenol -d5
Nitrobenzene-d5
2-Fluorobiphenyl
2,4 ,6-Tr i bromophenol
p-Terphenyl-d!4
ug/kg
<500
460
<500
<3300
360
<330
350
<330
<660
<660
<170
<170
<500
<330
<1700
<1700
<1700
<1700
<1700
<1700
<1700
<1700
<1700
<1700
<1700
<1700
<1700
<1700
<1700
<1700
<1700
Percent
65
70
65
97
35
72
ug/kg
<500
590
<500
<3300
360
<330
430
<330
<660
<660
<170
<170
<500
<330
<1700
<1700
<1700
<1700
<1700
<1700
<1700
<1700
<1700
<1700
<1700
<1700
<1700
<1700
<1700
<1700
<1700
Recovery (I)
55
65
58
89
15
69
-------
c-4;
Canonie
8704049
Page 2 of 3
Table 1. Semivolatile Organic Results
Canonie Sample ID
4-15-3 4-15-12
3351 3363
8270 Compounds ug/kg ug/kg
Phenol <170 <170
Bis(2-cnloroethyl)ether <170 <170
2-Chlorophenol <170 <170
1,3-Dichlorobenzene <170 <170
1,4-Dichlorobenzene <170 <170
1,2-Dichlorobenzene <330 <330
Bis(2-chloroisopropyl)ether <170 <170
N-Nitroso-di-n-propylamine <660 <660
Hexachloroethane <330 <330
Nitrobenzene <500 <500
Isophorone <330 <330
2-Nitrophenol <660 <660
2,4-Dimethylphenol <500 <500
Bis(2-chloroethoxy)methane <330 <330
2,4-Dichlorophenol <500 <500
1,2,4-Trichlorobenzene <170 <170
Naphthalene <170 <170
Hexachlorobutadiene <330 <330
4-Chloro-3-methylphenol <170 <170
Hexachlorocyclopentadiene <3300 <3300
2,4,6-Trichlorophenol <330 <330
2-Chloronaphthalene <170 <170
Dimethyl phthalate <170 <170
Acenaphthylene <170 <170
Acenaphthene <170 <170
2,4-Dinitrophenol <3300 <3300
4-Nitrophenol <1300 <1300
2,4-Dinitrotoluene <330 <330
2,6-Dinitrotoluene <500 <500
Oiethyl phthalate <170 <170
4-Chlorophenyl-phenyl ether <170 <170
Fluorene <170 430
4,6-Dim'tro-2-metnylphenol <990 <990
N-Nitrosodiphenylamine <660 <660
4-Bromophenyl-phenyl ether <170 <170
Hexachlorobenzene <500 <500
Pentachlorophenol <170 <170
Phenanthrene 1300 2400
Anthracene <170 350
Di-n-Butyl phthalate <330 <330
-------
C-48
Canonie
8704049
Page 3 of 3
Table 1. Semivolatile Organic Results (continued)
Canonie Sample ID
4-15-3 4-15-12
3351 3363
8270 Compounds
Fluoranthene
Pyrene
Butyl benzyl phthalate
3,3-Dichlorobenzidine
Benzo(a)anthracene
Bis(2-ethylhexyl)phthalate
Chrysene
Di-n-octyl phthalate
Benzo(b)fluoranthene
Benzo(k)fluoranthene
Benzo(a)pyrene
Indeno(l,2,3-cd)pyrene
Dibenzo( a, h) anthracene
8enzo(g,h,i)perylene
Alpha-BHC
Beta-BHC
Gamma-BHC
Delta-3HC
Heptachlor
Aldrin
Heptachlor epoxide
Endosulfan I
Dieldrin
4, 4 '-DDE
Endrin
Endosulfan II
4,4'-DDD
Endrin aldehyde
Endosulfan sulfate
4,4'-DDT
PCB's
Surrogates
2-Fluorophenol
Phenol -d5
Nitrobenzene-d5
2-Fluorobiphenyl
2,4,6-Tribromophenol
p-Terpheny1-d!4
ug/kg
<500
540
<500
<3300
330
<330
<170
"<330
<660
<660
310
<170
<500
<330
<1700
<1700
<1700
<1700
<1700
<1700
<1700
<1700
<1700
<1700
<1700
<1700
<1700
<1700
<1700
<1700
<1700
Percent
58
61
61
85
66
65
ug/kg
660
870
<500
<3300
510
<330
<170
<330
<660
<660
<170
<170
<500
<330
<1700
<1700
<1700
<1700
<1700
<1700
<1700
<1700
<1700
<1700
<1700
<1700
<1700
<1700
<1700
<1700
<1700
Recovery (X)
61
64
66
93
73
71
-------
C-49
Canom'e
8704055
Page 2 of
Table 1. Semivolatile Organic Results
Canonie Sample ID
4-16-4 4-16-7
8270 Compounds ug/kg ug/kg
Phenol <170 <170
Bis(2-chloroethyl)ether <170 <170
2-Chlorophenol <170 <170
1,3-Oichlorobenzene <170 <170
1,4-Dichlorobenzene <170 <170
1,2-Dichlorobenzene <330 <330
8is(2-chloroisopropyl)ether <170 <170
N-Nitroso-di-n-propylamine <660 <660
Hexachloroethane <330 <330
Nitrobenzene <500 <500
Isophorone <330 <330
2-Nitrophenol <660 <660
2,4-Dimethylphenol <500 <500
Bis(2-ch1oroethoxy)methane <330 <330
2,4-Dichlorophenol <500 <500
1,2,4-Trichlorobenzene <170 <170
Naphthalene <170 <170
Hexachlorobutadiene <330 <330
4-Chloro-3-methylphenol <170 <170
Hexachlorocyclopentadiene <3300 <3300
2,4,6-Trichlorophenol <330 <330
2-Chloronaphthalene <170 <170
Dimethyl phthalate <170 <170
Acenaphthylene <170 <170
Acenaphthene <170 <170
2,4-Dinitrophenol <3300 <3300
4-Nitrophenol <1300 <1300
2,4-Dinitrotoluene <330 <330
2,6-Dinitrotoluene <500 <500
Diethyl phthalate <170 <170
4-Chlorophenyl-phenyl ether <170 <170
Fluorene 330 330
4,6-D1nitro-2-methylphenol <990 <990
N-Nitrosodiphenylamine <660 <660
4-Bromophenyl-phenyl ether <170 <170
Hexachlorobenzene <500 <500
Pentachlorophenol <170 <170
Phenanthrene 2100 1500
Anthracene 260 <170
Di-n-Butyl phthalate <330 <330
-------
C-50
Canom'e
8704055
Page 3 of 3
Table 1. Semivolatile Organic Results (continued)
Canonie Sample ID
8270 Compounds
Fluoranthene
Pyrene
Butyl benzyl phthalate
3,3-Dichlorobenzidine
Benzo(a) anthracene
Bis(2-ethylhexyl) phthalate
Chrysene
Di-n-octyl phthalate
Benzo( b) f 1 uoranthene
Benzol k) fl uoranthene
Benzo( a) pyrene
Indeno(l,2,3-cd)pyrene
Dibenzo(a.h) anthracene
8enzo(g,h,i)perylene
Alpha-8HC
Beta-BHC
Gamma -BHC
Oelta-BHC
Heptachlor
Aldrin
Heptachlor epoxide
Endosulfan I
Dieldrin
4,4'-DDE
Endrin
Endosulfan II
4, 4 '-ODD
Endrin aldehyde
Endosulfan sulfate
4,4'-DDT
PCB's
4-16-4
ug/kg
<500
690
<500
<3300
430
<330
510
<330
<660
<660
<170
<170
<500
<330
<1700
<1700
<1700
<1700
<1700
<1700
<1700
<1700
<1700
<1700
<1700
<1700
<1700
<1700
<1700
<1700
<1700
4-16-7
ug/kg
<500
530
<500
<3300
350
<330
480
<330
<660
<660
<170
<170
<500
<330
<1700
<1700
<1700
<1700
<1700
<1700
<1700
<1700
<1700
<1700
<1700
<1700
<1700
<1700
<1700
<1700
<1700
Surrogates
Percent Recovery (X)
2 -Fluoro phenol
Phenol-d5
Nitrobenzene-d5
2-Fluorobiphenyl
2,4,6-Tribromophenol
p-Terphenyl-d!4
70
70
68
102
26
70
40
35
35
58
23
40
-------
C-51
Canonie
8704062
Page 2 of 3
Table 1. Semivolatile Organic Results
Canonie Sample ID
8270 Compounds
4-17-4
ug/kg
Phenol <660
Bis(2-chloroethyl)ether <660
2-Chlorophenol <660
1,3-Dichlorobenzene <660
1,4-Dichlorobenzene <660
1,2-Dichlorobenzene <1300
Bis(2-chloroisopropyl)ether <660
N-Nitroso-di-n-propylamine <2600
Hexachloroethane <1300
Nitrobenzene <2000
Isophorone <1300
2-Nitrophenol <2600
2,4-Dimethylphenol <2000
Bis( 2-chloroethoxy)methane <1300
2,4-Dichlorophenol <2000
1,2,4-Trichlorobenzene <660
Naphthalene <660
Hexachlorobutadiene <1300
4-Chloro-3-methylphenol <660
Hexachlorocyclopentadiene <13000
2,4,6-Trichlorophenol <1300
2-Chloronaphthalene <660
Dimethyl phthalate <660
Acenaphthylene <660
Acenaphthene <660
2,4-Dinitrophenol <13000
4-Nitrophenol <5300
2,4-Dinitrotoluene <1300
2,6-Dinitrotoluene <2000
Diethyl phthalate <660
4-Chlorophenyl-phenyl ether <660
Fluorene <660
4,6-D1n1tro-2-methylphenol <4000
N-Nitrosod1phenylam1ne <2600
4-Bromophenyl-phenyl ether <660
Hexachlorobenzene <2000
Pentachlorophenol <660
Phenanthrene 2500
Anthracene <660
Di-n-Butyl phthalate <1300
-------
C-51
Canonie
8704062
Page 3 of 3
8270 Compounds
Table 1. Semivolatile Organic Results (continued)
Canonie Sample 10
4-17-4
ug/kg
Fluoranthene <2000
Pyrene <1300
Butyl benzyl phthalate <2000
3,3-Oichlorobenzidine <13000
Benzo(a)anthracene <660
Bis(2-ethylhexyl)phthalate <1300
Chrysene <660
Di-n-octyl phthalate <1300
Benzo(b)fluoranthene <2600
8enzo(k)fluoranthene <2600
Benzo(a)pyrene <660
Indeno(l,2,3-cd)pyrene <660
Dibenzo(a.h)anthracene <2000
Benzo(g,h,i)perylene <1300
Alpha-BHC <6600
Beta-BHC <6600
Gamma-BHC <6600
Oelta-BHC <6600
Heptachlor <6600
Aldrin <6600
Heptachlor epoxide <6600
Endosulfan I <6600
Dieldrin <6600
4,4'-ODE <6600
Endrin <6600
Endosulfan II <6600
4,4'-ODD <6600
Endrin aldehyde <6600
Endosulfan sulfate <6600
4,4'-DDT <6600
PCB's <6600
Surrogates
2-Fluorophenol
Pheno1-d5
Nitrobenzene-d5
2-Fluorobiphenyl
2,4,6-Tribromophenol
p-Terphenyl-d!4
Percent Recovery (X)
65
57
38
82
9
62
9 - surrogate diluted below its detection limit
-------
Table 2
Results of Total Ext. Hydrocarbons Analysis on Soil
Samples Received From McKin
Results in mg/kg
04-08-198?
84-130-1840
Page 2
Sampler ID:
Lab 101:
Analyte(s)
Total Extractable Hydrocarbons
3-17-8
3992
702291
30.
Analyst Checked by
Note:
NO X denotes none detected to a level of X.
CaitonieEnvironmental
o
I
en
CO
-------
Table 2 03-30-1987
Results of TEH Analysis on Soil 84-130-1856
Samples Received From McKin Page 2
Results in mg/kg
Sampler 10: 3-20-12
Lab ID*: 702481
Analyte(s)
Total Extractable Hydrocarbons 58.
Analyst Checked by
Note:
NO X denotes none detected to a level of X.
o
I
CJ1
-------
Table 2 04-06-19o/
Results of Total Ext. Hydrocarbons Analysis on Soil 84-130-1885
Samples Received From McKin Page 2
Results In mg/kg
Sampler ID: 3-24 11 3-25-14 3-25-3
3700 3219 3206
Lab IDI: 702763 702765 702764
Analyte(s)
Total Extractable Hydrocarbons 55. 40. 47.
Analyst Checked by
o
I
Note:
tin v
-------
Table 2 04-08-1987
Results of Total Ext. Hydrocarbons Analysis on Soil 84-130-1912
Samples Received From McKin Page 2
Results in mg/kg
Sampler ID: 3-27-3
3279
Lab ID*: 703070
Analyte(s)
Total Extractable Hydrocarbons 39.
Analyst Checked by
o
I
N°te: , , r v r«~..~—5~TT ' - * *
NO X denotes none detected to a level of X.
-------
Table 2 04-08-1987
Results of Total Ext. Hydrocarbons Analysis on Soil 84-130-1926
Samples Received From McKin Page 2
Results In mg/kg
Sampler ID: 3-27-6 3-30-4
3244 3297
Lab IDI: 703156 703159
Analyte(s)
Total Extractable Hydrocarbons 28. 34.
Analyst Checked by
o
i
en
Note:
wn v
-------
Table 2 04-21-19o*
Results of Total Petroleum Hydrocarbon Analysis on Soil 84-130-1986
Samples Received From McKln Page 2
Results In mg/kg
Sampler ID: 4-14-4 4-14-13
3494 3495
Lab 101: 704064 704065
Analyte(s)
Total Extractable Hydrocarbons 120. 140.
r
Analyst Cheked by
denotes none detected to a level of X.
* -i _r v ^..a tn An Interfering peak.
r>
i
en
CO
-------
C-59
8705027
Page 2 of 2
Table 1. Total Extractable Hydrocarbon Results
Canonie Sample in
4-10-18 3324 3329 4-14-4 4-14-13
mg/Kg mg/Kg mg/Kg mg/Kg mg/Kg
TEH 130 180 100 200 170
-------
Table 2
Results of Total Petroleum Hydrocarbons Analysis on Soil
Samples Received From McKin
Results In mg/kg
04-27-1987
84-130-2009
Page 2
Sampler ID:
Lab ID*:
Analyte(s)
TotaTTxtr act able Hydrocarbons
4-15-14
3365
704358
190.
4-15-8
3356
704357
120.
4-16-16
3386
704360
220.
4-16-4
3372
704359
130.
4-17-12
3400
704361
140.
Analyst Checked by
o
I
crv
Note:
-------
C-61
Canonie
8705064
Page 2 of 2
Table 1. Total Organic Hydrocarbon Results
Concentration
Sample Identification
3-18-3
3-19-3
3-19-15
3-23-3
3-23-11
3-26-2
3-26-5
4-2-3
4-2-14
4-3-6
4-3-13
4-7-8
4-8-7
4-8-9
4-9-4
4-9-13
4-14
4-15
4-14-4
(mg/kg)
47
73
<10
20
<10
20
16
110
280
180
200
150
100
350
370
200
80
160
190
-------
APPENDIX D
QUALITY ASSURANCE DATA -
McKIN/STOCKTON, CA
LABORATORY ANALYTICAL COMPARISON
CanonieEnvironmenta!
-------
D-l
MEMO
TO: Brian Bell CH 84-130
FROM: Karen Verrue^? -June 8, 1987
QA Data. McK1n Prolect
Enclosed are the plots of the relative percent difference (RPD) for all the
analytes Investigated by EPA method 8010/8020 for the McK1n project 1n Gray,
Maine.
Originally, samples were analyzed on-s1te, then the sample was shipped to
the laboratory In Stockton, California, and analyzed. It was determined
that In shipping the sample, a substantial amount of the contaminates were
lost due to the fact that a head-space was created 1n the sample tube when
the original analysis was performed and due to the fact that the sample was
extracted at the on-s1te lab within hours of sampling, whereas the sample
was extracted at the Stockton lab seven to ten days later.
Sample extracts were then shipped for analysis to the laboratory 1n
Stockton, after the analysis was completed on-s1te.
The overall comparison of the data shows agreement between the two analyses
1n regards to Identification and relative amounts. Towards the end of the
project, results from the laboratory 1n Stockton were running higher than
those found on-s1te. Based on the EPA proficiency samples analyzed at the
site 1n Gray, Maine, and at the lab 1n Stockton, the problem was not with
the analytical work. We feel that the higher results were due to the sample
matrix; the samples taken towards the end of the project contained a large
amount of an oily substance. Over time, we feel that more of the
contaminates leached or were extracted Into the methanol.
If you need any more Information, please give me a call.
KAV/Jmh
Enclosure
cc: Ken Hahl
CanonieEnvironme
-------
D-2
q
d
a
Canonie Environmental Services - McKin/Stockton Comparison
0»ff«r«ne» for 1,2-OicH«rMth»r»
3D
J
18
17 -)
16 -
IS -
14 -
12 -
11 -
10 H
a
7
6
5
4
3
2
1
O
.3/4/36 8/15/86 »/22/a* 11/5/8611/25/861
DotoSorptod
1/2»/87 3/25/87
Analytt:
Lab ID:
DaU:
fcKin Val«:
Stockton Vtli
R.P.D.:
1,2-DichlorovthfM
PS 16-LJ1
3/4/86
ND 11
ND 11
i.
7-21-1
7/21/86
ND IK
ND8.82
1
7-38-1
7/38/86
ND8.K
NO 8. 88
8.
8-15-1
8/13/86
ND 8.K
N08.K
8.
8-29-1
8/29/86
ND IK
NO 8.82
1
9-12-218
9/12/86
ND 184
ND8.82
1
9-22-Hol
9/22/86
ND 11
NO 8.2
1
Lab 10: 18-21-13
Oitt: 18/21/8*
MeKiR Val«: NO 8.82
Stockton Valuii • 192
R.P.O.: 8.
18-27Hol327 11-91126
18/27/81 11/5/86
NO 8.12 NO 8.82
NO M2 NO 8.82
8. 8.
11-12H0133S
11/12/tf
W8.1
MD 8.2
8.
ll-13Hol351
11/13/86
NO 8.82
ND 8.82
8.
11-25H01428
11/237 8i
NO 8.82
ND8.82
I.
12-lHolf4*3
12/1/86
NO 8.82
ND 182
8.
1,2-lidtlora
Lab ID: 12-18-7
Datt: 12/18/16
fcKin Val«t « 8.K
Stodttm Vilu»: ND8.82
R.P.O.: 1
12-16-3
12/16/86
NO IK
ND8.82
8.
12-31A1STP
12/31/86
ND IK
ND8.82
1
1-13 Art* 6 1-29M-12 2-3-11
1/13/87 1/29/87 2/3/87
25. ND 182 ND 8.K
24. NO 8.82 ND 8.82
4.1 8. 8.
Vtl
ND 8.82 fto4t.
8. IP.li
i/a/87
• lie
• IK
I.
CanonieEnvironmentdl
-------
ff £*£
9. 5 - S
»• * 5 B-ST
P 8 5 S »
P S • " 3
- 9 s *
R.P.D.
I
o
9
8 85 Jjl
?» f» S Sf
B n> g» -.j
S 8 B t
5 *g§
«•» c s
K» K tS
P« 2K *~ •*
® "*•
8C! V
>• w f r c f
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• £ - *
£i
U
W
.- e
S 8K
f ^
C *
^* * ^ Cjii
o» • S3
5* * • w
* *• W
i
3
I
-------
D-4
o
a
ei.
Canonic Environmental Services - McK in/Stockton Comparison
20
19
13
17
16
IS
14
12
11
10
9
8
7
6
S
4 -
« for 1 ,
(»—•-
3/4/1
RMlyti:
1,3-Dichlorobtnwnt
Lab 11:
Datt:
fcKin Val«i
Stockton ValtM:
R. P.O.:
Lab ID:
Ditit
McKiit Valuis
Stockton Valwi
IP.O.j
Lab IBs
Datt:
*Kin Valwi
Stocttoa Viluii
IP.D.J
PS 1HJ1
3/4/86
18.
« 18.
8.
18-21-13
10/21/81
ID 0.82
•> 102
*•
12-18-7
12/10/86
• 0.02
•00.02
8.
7-21-1
7/21/86
NO 8.02
NO 0.82
0.
10-e7Hol327
10/27/81
NO 0.02
NB 0.2
*•
12-16-3
12/16/86
NI0.02
NO 0.02
0.
7-38-1
7/38/86
NO 8.02
108.82
8.
11-SI126
11/5/S6
NO 0.02
» 0.02
0.
12-31WSTP
12/31 /K
W 8.02
NO 0.02
0.
8-15-1
6/15/86
« 8.02
NO 0.02
6.
11-12H01339
11/12/81
NO 0.1
M0.2
0.
1-13 Ana 6
1/13/67
• 0.04
NO 0.04
8.
8-29-1
6/29/86
W0.02
NO 0.02
0.
ll-13Nol331
11/13/86
NO 0.02
ND0.02
0.
14M-12
1/29/87
« 0.02
NO 0.02
0.
9-^216
9/12/86
« 8.04
NO 0.02
0.
11-25H01420
11/25/81
NO 0.02
« 8,02
0.
^3-^
2/3/67
NB 0.02
NO 0.02
0.
9-22-Holtdl
9/22/86
Ni 8.1
NO 0.2
0.
12-lHolt443
12/1/86
NO 0.82
m 8.02
0.
3-18-7
3/18/67 L* i><
W 8.02 J*«
NO 0.82 *Mt.
1. IP.«.:
l,3-0idilapo
1/2V81
Vil«: IDI.K
v«l«: « 1M
I.
CanomeEnvironmentdi
-------
D-5
a
si
4
Canonie Environmental Serv-ices - McKin/Stockton Comparison
Mctiw* PMC** OfffarwK* for 1.4-Oie Horcb»n»r»
!0 -O
n/s/ae
DotoSvrptod
t/a»/«7 j/as/87
1,4-Oicfilorobmai*
Lab 10: PS 16-LJ1 7-21-1
Datt: 3/4/86 7/21/86
IfcKin Valus 38. « 0.02
Stockton Valuts 42. NO 0.02
I P.O.: 18. 8.
7-30-1
7/38/86
W 0.02
100.02
8.
8-15-1
6/1S/86
M 8.02
NO 0.02
1
8-29-1
6/29/86
m 8.02
NO 0.02
8.
9-12-210
9/12/86
* 8.04
NO 0.82
8.
9-22-Holt0<
9/22/86
* 8.1
NO 0.2
0.
Lab ID] 18-21-13
Oatt: 18/21/81
Mddn VilutJ NO 8.82
Stodcton Val«i • H02
R.P.O.: 8.
l«7Ho!327
18/27/H 11/5/86
HO 0.82 NO 8.82
Ml 0.2 m 8.02
8. 8.
11-12H0133S 11-13H013S1
11/12/86 11/13/86
NO 0.1 100.82
N8 8.2 » 8.02
0. 8.
11-23H01428 12-lNolt443
11/23/K 12/1/86
NO 0.82 NO 0.82
• 8.02 W 8.02
8. 0.
Lab III 12-18-7
Datt: 12/18/86
NeKin Val«> • 0.02
Stocktoa Viluii 100.02
I. P.O.: 8.
12-16-3
12/16/06
Ml 0.82
NO 0.02
8.
. 12-31A1STP
12/31 /K
NO 8.2
ND0.2
8.
l-13flrttB 1-29B-13
1/13/87 1/29/1?
« 8.04 M) 8.02
NO 0.84 NO 0.02
8. 8.
2-3-11
2/3/17
m 102
NO 8. 82
1
3-18-7
3/10/67 "
* 102 JJ
NO 0.02 »
0. ll
til
3-O-*
V2V87
v
ID
CanonieEnvironmentdi
-------
D-6
Canonic Environmental Services — McKin/Stockton Comparison
Rrtattw* Parmrt Oiff««rc« for I
«O
SO -
Q
a
a
1O -
3/4/86 8/15/1
flnalytt:
Lib ID: PS 16-LJi
Ditt: 3M/86
NcKin Vil«t » 90.
Stock** Vtl«: NO 588.
R.P.D.: 1
7-ai-i
7/21/46
» 1.
NDt.2
1.
7-31-1
7/N/K
« 1.
«i.e
1.
8-15-1
8/15/K
« 1.
NDI.a
1.
8-29-1
8/29/86
« 1.
»ie
8.
9-12-218
9/12/86
« 5.
«2,
8.
9-22-Hol«2N
9/28/86
« S
mi.
8.
Lab 10: 18-21-13 11-91126
Date 18/21/M 11/5/84
He*in Vilwi » 1. N> 1.
Stockton Val«i N) 8.2 W 8.2
R.P.D.I 8. 8.
11-I3HL3S1 ll-2SHOL42a 12-1HOL443 12-18-7 12-16-3
11/13/8S 11/29/8& 12/1/86 12/18/8S 12/1&/M
Ml. N) 1. NO 1. « 1. ND 1.
1.7 * 8.2 W 8.2 * 8.2 W 8.2
92. 8. 8. 8. 8.
Lab It!
Data:
fcKin Valwt
StocktwViluit
I P.O.:
12-3101STP l-13flrw«
12/31 /ft 1/13/87
8.7 «&
RD2. m 1.
8. 8.
1-29A6-12
1/29/87
« 1.
• 8.2
8.
2-3-11
2/3/87
« 1.
• 8.2
8.
3-18-7
3/16/87
M)8.S
«8.2
8.
3-29-9
3/25/87
NB8.5
HO 8,2
8.
*-3-S
4/3/r
• 8.S
NB8.2
8.
CanonieEnvironmentdi
-------
D-7
Canonic Environmental S
19O
ervices - McK in/ Stockton Comparison
*rt Oiftar«nc* for
p
0.
a
0 HI—•—•
3/4 /as a/i6/a« a/aa/ae
12/31/as 2/3/B7
DotoSorptad
AMlytt]
Ethylbmzt
Uta II:
Oattj
NeKin Vil»j ND
Stocttot Vilwi ND
LP.O.: 8.
PS 16-LJ1
3/4/86
7-21-1
7/21/86
ND 1.
NO 8.2
8.
7-38-1
7/98/86
NB 1.
NO 8.2
8.
8-15-1
8/1S/86
ND 1.
ND8.2
8.
8-29-1
8/29/86
ND 1.
ND8.2
8.
9-12-218
9/12/86
NDS.
ND2.
8.
9-22Holt»
9/22/86
189.
ND 2.
198.
Lab IDs lt-ei-13
tattt
HcKifl VUg,, » 1.
Sto<*t« Valwt 0 1
R.P.O.: «.
11-M126 11-12HOL339 11-13HDL3S1
11/5/86 ll/12/8f 11/13/86 11/25/81
ND1. 14. 5. 8.49
8.4 41 9.1 8.4
8. 183. 38. 28.
1MHDLH3 12-11-7
12/1/86 12/11/81
1.7 « 1.
1.9 M) 1.2
6& t.
Ethyl
Lib III 12-16-3
tatci 12/16/86
NcKtn talm ND 1.
Stechtoi Vila i ND 1,2
I. P.O.: 1
12-31A1STP l-!3flr«a
12/31 /K 1/13/87
3.7 5.
28. 8.
IS. 46.
l-29flft-12
1/29/87
M) 1.
W8.2
8.
2-3-11
2/3/87
m i.
• 8.2
8.
3-18-7
3/18/87
NB8.S
NO 8.2
8.
3-23-9
3/29/87
• 8.5
NB8.2
8.
Itelytn
Uk lit
ktti 4/3/1
NMil Vlltti • ••
*ofttn Vtlwt » 1
I P.O.: 1
CanonieEnvironmerlai
-------
D-8
Canonic Environmental Services — McKin/Stockton Comparison
a
i
a
230
'86 8/IS/86 0/22/86 11/5/86 11/23/86 12/1 «/•* 1/29/17 3/26/87
Kb II: PS 16-111 7-21-1
Dittt 3/4/86 7/21/86
NeKin Vilwi NO It MB 8.02
Stockton WINK * 18. NO 8.88
R.P.O.! 8. 8.
7/31/86
NBM2
NO 8.82
8.
8/1S/86
NDS.I2
ND8.82
8.
8/Z9/K
NO 8. ft
8.
9-12-218
9/22/86
8. SI
1.1
9/22/86
11.1
NO 8,2
199.
Lab IPt 11-21-13
bti: ll/21/at
NcKin Valutt 10 I.tt
Stoditm Valw: * itt
R.P.D.: I.
•.«
Nia
67.
i.e
iia
46.
11-12H0133S ll-13Hol351
11/12/86 11/13/86 11/23/8*
NO 8.1 NO 8.82 ND 1.82
« 8.2 NO 0.6* 8.83
8. 8. 48.
12/1/86
ND 9.82
« 8.82
8.
Kb III 12-18-7 12-16-3 12-31A1JTP 1-13 Art* 8
Oatti 12/18/86 12/16/86 12/21/86 1/13/87
NcKin «•!•: Nf 8.82 NO 8.82 NO 8.82 ND 8.84
StocMn Vdot 108.82 NO 8.82 ND8.82 NO 8.84
tP.O.: t I. I. 8.
i-2»8-12 2-3-11 3-18-7
1/29/67 2/3/17 3/18/67
« 8.82 MB 8.82 « 8.82
NO 8.82 NO 8.82 NO 8.82
8. 8. 8.
Ltt III
Inn
M«II Vtl«i
•otttv ««!
IP.t. i
Ti»ri
3-ff-f
1/2S/I7
ID •••
« 4*2
t.
«/.
10
Mil
4.
CanonieEnvircni
-------
D-9
Canonic Environmental Services - McKin/Stockton Comparison
Dat«tiv» ^rc*ii Dftaranc* tor 1,1,1 -TrichtorMtharw
90
a
2.
so -
70 -
eo -
so -
« -
30 -
30 -
10 -
O ^••^
a/is./as
DotoScrrptad
Aulytt:
1,1,1-Tridilororthmt
Lab 10: PS 16-LJ1
Oati: 3/4/86
fcKin Val«i ft It
Stockton Vilut: ND 18.
I.P.O.: I.
7-21-1
7/21/86
ft 8.02
NO 8. 82
8.
7-38-1
7/38/86
NO 0.82
ND8.82
8.
8-15-1
8/1S/86
NO 8.82
ND8.82
8.
8-29-1
8/29/86
ND 8.82
ND8.82
8.
9-12-218
9/22/86
ft 8.84
NO 8. 82
8.
9-22-Holt2N
9/22/86
8.1
NO 8.2
8.
Lab ID: 11-21-13
Ditfi ll/21/a
NcKU Vtluii B) •.«
Stoditon Val«i It
R.P.D.: i,
lf/£7/8f
«0 8.12
Ml e.12
t.
11/5/86
ND Lie
ND 1.12
t.
H-12Hol33S tl-l3Hol351 1
11/12/86 11/13/86 11/25/86
ND8.1 NO 8.82 ND8.82
ND 8.2 * 8.82 ft 8.82
8. 8. 8.
12-Wtelt443
12/1/86
NO 8.82
8.82
I.
Ub lit 12-18-7
Datti 12/11/86
fcKin tal«i m 8.02
Stocttcn Vil*: NO 8.82
I. P.O.: 8.
12-16-3
12/16/86
0.83
ND8.82
44
12-31AWTP
12/31/86
ft 8.02
NO 8. 82
1.
1-13 Art* 8
1/13/87
NB8.84
NO 8. 84
8.
1-29M-12
1/29/87
ND8.82
8.89
86.
2-3-11
2/3/17
ft 8.82
NO 8. 82
8.
3-18-7
3/18/87
ft 8.82
NO 8.82
8.
toirttt
Uk IDi
MM
Mil Vittot
Boat* *•!•:
tP.0.1
1.1. 1-T'
3-e-i
J/»W
IDI.K
I.U
««.
CanonleEnviroimentdl
-------
0-10
Canonie Environmental Services - McKin/Stockton Comparison
FMatN* Parcant OH«wnc» far
200
q
a.
a
Tridilorotthylw*
Lab Ih
Oatt:
McKin Valut:
Stocktot V»l«t
R.P.O.: 55.
PS I6-LJ1
3/4/86
378.
7-21-1
7/21/86
M 102
7-38-1
7/38/86
N8182
ND0.02
8-15-1
8/15/86
ND102
HD0.82
1
8/29/86
NB) « *2
NO 8.82
1
9/12/06
17.4
69.
119.
9/22/86
125.
ND12
280.
Lab ID: 18-21-13
Dtt« 18/21/tt
HcKii Vilw: 8.22
Stoditon Vjlutj 1 IS
R.P.O.: 38.
18-87Hol327 11-W126
lf/27/ai 11/V66
61. 1.9
38. 1.8
46. 62.
11-12H0133S
11/12/86
6.5
7.5
14.
11-13H»1351
11/13/86 11/23/16
2.1 8.86
2.3 8.11
9.1 39.
12/1/86
8.24
123
4.
Lab IB: 12-18-7
Date: 12/18/86
fcKin Valut: 10 0.02
Stodrtoi 0.82
8.
12-31A1STP
12/31/86
ND 182
ND0.82
1
1-13 ATM
1/13/87
8.07
ND0.84
54.
18 1-29M-12
1/29/87
• 102
ND0.82
1
2-3-U
2^/87
• 102
NO 0.02
1
3-18-7
3/10/87
104
0.83
29.
Miiym
Uk Hi
turn
miu va«i
iriaia
3-iM
3/31/67
i.
CanonieEnvircnmental
-------
D-ll
Canonic Environmental Services - McKin/Stockton Comparison
Ftrcant Offaranc* for Tdu»n»
Q
a.
o -<»
.3/4/86 8/1S/
tealytt:
Ub ID:
Datt:
fcKin Val«i
Stocktm Vtli
R.P.D.:
Toluiiw
PS 16-LH
374/16
M> SM.
»SM.
i.
7-ai-i
7/21/66
« 1.
NBI.Z
1.
7-3»-l
7/31/86
• 1.
NDI.Z
1.
8-15-1
8/15/86
« 1.
• 1.2
t.
8-29-1
8/39/86
« 1.
• 1.2
8.
9-12-211
9/12/86
MS.
»2.
8.
9-22-Holt»
9/22/86
m s.
mz.
8.
Lab ID: 18-21-13 11-MUS
Ditii 18/21/81 11/9/86
Mdtin Vilut: Ml 1. Ml.
Stodtton Valw: It 13 NB 8,2
R.P.O.: 8. 8.
11-12HOL33S 11-13HDL351 11-290.428 12-1HOL443 12-18-7
11/12/8S 11/13/86 11/2S/8S 12/1/86 12/18/86
IS. 5. 8.38 3.8 18) 1.
41 11. 8.3 1.8 » 8.2
96. 75. 24. 181. 8.
•jtlyttt
Lab IB:
Data:
fcKin Valui:
Stockton Vtlui
R.P.O.:
12-16-3
12/16/86
» 1.
ti ND8.2
8.
12-31A1STP
12/31/81
18
8.
96.
l-13taNA
1/13/87
3.
16.
137.
1-29*8-12
1/29/87
» 1.
NO 8.2
1
2-3-11
2/3/87
• 1.
8.4
8.
3-18-7
3/18/87
(8)8.3
NO 8.2
8.
3-25-9
3/29/87
• 8.5
NO 8.2
8.
Uk lit
htH
•fj^i_ u,
^D\1V ~
Stodta
LP.O.I
Tol
4-3-9
4/3/17
NOI.S
« 13
I.
CanonieEnvircnmentd!
-------
D-12
Canonic Environmental Services — McKin/Stockton Comparison
F*rc«r* DHmnc* tor
200
a
a
a
flMlyti:
Xyl
Lab 10:
Oati:
NcKin Val«:
Stockton Vtlwi
R.P.O.:
PS 16-LM
3/4/86
ND 5*8.
ND588.
8.
7-21-1
7-38-1
7/21/86 7/38/86
ND
NO
8.
i.
8X2
m
m
8.
1.
8.2
8-15-1
8/15/86
N)
NO
8.
1.
8.2
8-29-1 9-12-218 9-22-Hol
8/29/86
ND
NO
8.
1.
8.2
9/12/86
12.6
188.
139.
9/22/86
448.
3.1
197.
Lab ID:
DitK
NcKin Valw:
Stodtt«n ValM
R.P.O. :
18-21-13
18/21/fli
18) 1.
t » 8.£
8.
11-* 126
11/3/86
MM.
8.4
8.
11-12HOL335 U-13HXJS1 ll-25HOL42i
11/12/84 11/13/tf 11/23/8S
69. 22. 1.9
131. 27. 2.1
61. ». II.
12-1HOL443 12-11-7
12/1/86 12/11/86
9.2 A 1.
4.5 * US
69. 1
lyli
Ub IDi 12-16-3
Datt: 12/16/86
NcKin Valut: m 1.
Stockton Valuu NO 1.2
R.P.D.: I.
12-31A1STP
12/31/86 1/13/87
32. 15.
81. 37.
87. 66.
1-29R8-12
1/29/87
« 1.
ND8.2
8.
2-3-n
2/3/87
18)1.
NO 8.2
8.
3-18-7
3/18/87
• 8.3
NO 8.2
8.
3-25-9
3/25/87
18)8.5
NO 8.2
8.
lafe tit 4-3-5
8tt« 4/3/17
fcKu VU«i ND I.S
StocktM «!•> * 12
K.P.O. i 1.
CanonieEnvircnmentdi
-------
APPENDIX E
COMPARISON OF PRE-TREATMENT AND POST-TREATMENT
SOIL CHARACTERIZATION - SOILS CONTAINING VOC'S
CanonieEnvironmeri
-------
E-l
COMPARISON OF'PRETREATMENT AND POST-TREATMENT SOIL CHARACTERIZATION
LOW TEMPERATURE THERMAL AERATION PROCESS
MCKIN SUPERFUND SITE
GRAY, MAINE
SAMPLE I.D.
Type
31368.9
Pretreatment
31368.9
Post-treatment
31683.9
Pretreatment
3168:
Po«t-ti
U.S. EPA Method 8020
Benzene
Chlorobenzene
1,2-Dichlorobenzene
1,3-Dichlorobenzene
1,4-Dichlorobenzene
Ethylbenzene
Toluene
Xylenes-
U.S. EPA Method 8010
Bromodichlororaethane
Bromoform
Bromome thane
Carbon Tetrachloride
Chlorobenzene
Chloroethane
2-Chloroethylvinyl ether
Chloroform
Chloromethane
Dibromochlorotnethane
1,2-Dichlorobenzene
1,3-Dichlorobenzene
1,4-Dichlorobenzen«
Dichlorodifluororaethan*
1,1-Dichloroethane
1,2-Dichloroethane
1,l-Dichloroethen«
trans-1,1-Dichloroethene
1,2-Dichlorppropane
ci«-l,3-Dichloropi
trans-1,3-Dichloropropene
1,1,2,2-Tetrachloroethane
Tetrachloroethane
1,1,1-Trichloro*than«
1,1,2-Trichloroethan«
Trichloroethpne
Trichlorofluoromethane
Vinyl chloride
Mcthylen* chloride
Location 1
NO 10.
Location 2
NO 0.02
NO 0.02
NO 0.02
NO 0.02
NO 0.02
NO 0.02
NO 0.02
NO 0.02
NO 0.02
NO 0.02
NO 0.02
NO 0.02
NO 0.02
NO 0.02
NO 0.02
NO 0
NO 0.
,11
02
02
0.
NO 0.02
NO 0.02
NO 0.02
NO 0.02
0.09
0.13
NO 0.02
7.3
NO 0.02
NO 0.02
NO 0.02
NO 1,
NO 1
NO 1
NO 1
NO 1
28
35
84
NO 0.02
NO 0.02
NO 0.02
NO 1.
NO 1.
NO 1.
NO 0.02
NO 0.02
NO 0.02
NO 0.02
NO 0.02
NO 0.02
NO 0.02
NO 10.
NO 0.02
NO 0.02
NO 0.02
NO 10.
16
20
38
NO 0.
NO 0,
NO 0,
02
02
02
NO 0.02
NO 0.02
NO 0
0
NO
NO 0.
NO 0.
NO 0.
NO 0.
NO 0,
NO 0,
02
02
02
02
02
02
02
02
16
NO 0.02
NO 0.02
NO 0.02
0
0
0
NO
NO
NO
NO
02
02
02
0.02
NO 0.
NO
02
0.04
0.02
20
NO 0.02
NO 0.02
NO 0.02
NT
NC
NI
ND
NC
ND
ND
ND i
ND i
ND I
ND I
ND (
ND (
Note: All values shown are in mg/kg.
ND x indicates that compound was not detected at a concentration in excess of
x mg/kg. Where no value is reported for a particular compound, that compound
was not analyzed in post-treatment .soil samples.
-------
E-2
COMPARISON OF PRETREATMENT AND POST-TREATMENT SOIL CHARACTERIZATION
LOW TEMPERATURE THERMAL AERATION PROCESS
MCKIN SUPERFUND SITE
GRAY, MAINE
(Continued)
SAMPLE 1.0.
Type
U.S. EPA Method 8020
Benzene
Chlorobenzene
1,2-Dichlorobenzene
1,3-Dichlorobenzene
1,4-Dichlorobenzene
Ethylbenzene
Toluene
Xylenes
U.S. EPA, Method 8010
Bromodichloromethane
Bromofonn
Bromomethane
Carbon Tetrachloride
Chlorobenzene
Chloroethane
2-Chloroethylvinyl ether
Chloroform
Chloromethane
Dibromochloromethane
1,2-Oichlorobenzene
1,3-Dichlorobenzene
1,4-Dichlorobenzene
Dichlorodifluoromethane
1,1-Dichloroethane
1,2-Dichloroethane
1,1-Dichloroethen*
trans-1,1-Dichloroethene
1,2-Dichloropropane
cis-1,3-Dichloropropene
trans-1,3-Dichloropropene
1.1,2,2-Tetrachloroethane
Tetrachloroethane
1.1,1-Trichloroethane
&1,1,2-Trichloroethane
Trichloroeth%ie
Trichlorofluororoethane
Vinyl chloride
Methylene chloride
32083.5
Pretreatntent
32083.5
Post-treatment
Location 3
ND 5.
ND 0.1
ND 0.1
ND 0.1
ND 5.
300
130
840
ND 0.1
ND 0.1
ND 0.1
ND 0.1
ND 0.1
ND 0.1
ND 0.1
ND 2
ND 0.1
ND 0.1
ND 0.1
ND 0.1
ND 0.1
ND 0.1
ND 0.1
ND 0.1
ND 2
ND 0.1
ND 0.1
ND 0.1
ND 0.1
ND 0.1
ND 0.1
ND 0.1
ND 0.1
300
40
1.1
650
ND 1.
ND 0
ND 0
ND
02
02
0.02
ND
ND
ND
1.
1.
1.
ND 0.02
ND 0.02
ND 0.02
ND 0.02
ND 0.02
ND 0.02
0.04
32077.5
Pretreatment
32071
Ppst-trei
Location 4
ND 10.
ND 0.2
ND 0.2
ND 0.2
ND 10.
ND 10.
ND 10.
15
ND 0
ND 0
ND
ND
ND
ND
ND
ND
ND
ND
0.
0.
0.
0,
0,
ND
ND
ND
ND
ND
ND 0
ND 0
ND 0
ND 0
ND 0
2
,2
.2
.2
,2
.2
.2
.2
.2
.2
2
2
2
2
2
2
2
,2
,2
.2
15
ND
ND
ND
ND
ND
0.35
2
2
2
0.54
,2
,2
0.53
ND 1.
ND 0
ND 0
ND 0
ND 1
ND 1
ND 1
ND 0.0,
ND 0.0:
ND o.o;
ND o.o;
ND o.o;
ND o.o;
0.04
Note: All values shown are in mg/kg.
ND x indicates that compound was not detected at a concentration in excess of
x mg/kg. Where no value is reported for a particular compound, that compound
was not analyzed in post-treatment soil samples.
-------
E-3
COMPARISON OF PRETREATMENT AND POST-TREATMENT SOIL CHARACTERIZATION
LOW TEMPERATURE THERMAL AERATION PROCESS
MCKIN SUPERFUND SITE
GRAY, MAINE
(Continued)
SAMPLE I.D.
Type
U.S. EPA Method 6020
Benzene
Chlorobenzene
1,2-Dichlorobenzene
1,3-Dichlorobenzene
1,4-Dichlorobenzene
Ethylbenzene
Toluene
Xylenes
U.S. EPA-Method 8010
Bromodichlororoethane
BrotnofortB
Broraomethane
Carbon Tetrachloride
Chlorobenzene
Chloroethane
2-Chloro«thylvinyl ether
Chloroforn
Chloromethane
Dibromochloromethane
1,2-Dichlorobenzene
1,3-Dichlorobenzene
1,4-Dichlorobenzene
Dichlorodifluoromethane
1,1-Dichloroethane
1,2-Dichloroethane
1,1-Dichloroethene
tran«-l,1-Dichloroethene
1,2-Dichloropropane
cis-1,3-Dichloropropene
tran«-1,3-Dichloropropene
1,1,2,2-Tetrachloroethane
Tetrachloroethan*
1,1,1-Trichloroethane
1,1,2-Trichloroethane
Trichloroethene
Tr ichlorofluoromethane
Vinyl chlorid*
M«thyl«n« chlorid*
32073.5
Pr«triatn»nt
32073.5
Po§t-tr«atB>«nt
Location 5
ND 10.
ND 0.2
ND 0.2
ND 0.2
ND 10.
43
19
ND 0.2
ND 0.2
ND 0.2
ND 0.2
ND 0.2
ND 0.2
ND 0.2
ND 0.2
ND 0.2
ND 0.2
ND 0.2
ND 0.2
ND 0.2
ND 0.2
ND 0.2
NO 0.2
ND 0.2
ND 0.2
ND 0.2
ND 0.2
ND 0.2
ND 0.2
ND 0.2
ND 0.2
43
8.8
0.4
210
ND 0.2
ND 1.
ND 0.02
ND 0.02
ND 0.02
ND 1.
ND 1.
ND 1.
ND 0.02
ND 0.02
ND 0.02
ND 0.02
ND 0.02
ND 0.02
0.04
32068.5 32068.
Pr«tr«atm«nt Post-treat
Location 6
ND 1.
ND 0.02
320
ND 0.02
ND 0.02
72
ND 1.
160
ND 1.
ND 0.
ND 0.
ND 0.
ND 1.
ND 1.
ND 1.
ND 1
ND 1
ND 1
ND 1
ND 1
ND 1
ND 1
ND 1
ND 1
ND 1
ND 1
ND 1
ND 1
ND 1
ND 1
ND 1
ND 1
ND 1
ND 1
ND 1
ND 1
ND 1
ND 1
320
6.1
120
19
3310
3.8
ND 0.0
ND 0.0
ND 0.0
ND 0.0:
ND o.o;
ND o.o:
Note: All values shown are in rog/kg.
ND x indicates that compound was not detected at a concentration in excess of
x mg/kg. Where no value is reported for a particular compound, that compound
was not analyzed in post-treatment soil samples.
-------
E-4
COMPARISON OF PRETREATMENT AND POST-TREATMENT SOIL CHARACTERIZATION
LOW TEMPERATURE THERMAL AERATION PROCESS
MCKIN SUPERFUND SITE
GRAY, MAINE
(Continued)
SAMPLE I.D.
Type
U.S. EPA Method 8020
Benzene
Chlorobenzene
1,2-Dichlorobenzene
1,3-Dichlorobenzene
1,4-Dichlorobenzene
Ethylbenzene
Toluene
Xylenes
U.S. EPA Method 8010
Bromodichloromethane
Bromoforo
Bromomethane
Carbon Tetrachloride
Chlorobenzene
Chloroethane
2-Chloro«thylvinyl ether
Chloroform
Chloromethane
0 ibromochloromethane
1,2-Dichlorobenzene
1,3-Dichlorobenzene
1,4-Dichlorobenzene
Dichlorodifluorotne thane
1,1-Dichloroethane
1,2-Dichloroethane
1,1-Dichloroethene
trans-1,1-Dichloroethene
1,2-Dichloroprop«M
ci«-1,3-Dichloropropene
trans-1,3-Dichloropropene
1,1,2,2-Tetrachloroethane
Tetrachloroethan*
1,1,1-Trichloroethane
1,1,2-Trichloroethane
Trichloroethene
Trichlorofluoromethane
Vinyl chloride
M«thyl«n« chloride
32365.3
Pretreatment
32365.3
Post-treatment
32483.5 324G
Pretreatment Post-tr<
Location 7
2.7
ND 0.02
33
ND 0.02
ND 0.02
1.8
4
12.9
ND
ND
ND
ND
ND
ND
ND
ND
ND 4
ND <
ND 4
ND 4
ND 4
ND
ND
ND
ND
ND
ND
ND
ND
L
I
33
I
I
I
,
4.3
8.6
ND 4
1000
ND
ND
ND
ND 1.
ND 0.02
ND 0.02
ND 0.02
ND 1.
ND 1.
ND 1.
ND 0.02
ND 0.02
ND 0.02
ND 0.02
ND 0.02
ND 0.02
ND 0.02
Location 8
ND 100
ND 2
ND 2
ND 2
ND 1
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
31
130
140
2
2
2
2
2
2
2
2
2
2
2
2
2
2
2
2
2
2
2
2
2
2
2
2
2
30
19
140
12
N
ND
ND
ND
ND
ND
ND
ND I
ND (
ND <
ND (
ND (
ND (
ND C
Note: All values shown are in mg/kg.
ND x indicates that compound was not detected at a concentration in excess of
x mg/kg. Where no value is reported for a particular compound, that compound
was not analyzed in post-treatment soil samples.
-------
E-5
COMPARISON OF PRETREATMENT AND POST-TREATMENT SOIL CHARACTERIZATION
LOW TEMPERATURE THERMAL AERATION PROCESS
MCKIN SUPERFUND SITE
GRAY, MAINE
(Continued)
SAMPLE I.D.
Type
U.S. EPA Method 8020
Benzene
Chlorobenzene
1,2-Dichlorobenzene
1,3-Dichlorobenzene
1,4-Dichlorobenzene
Ethylbenzene
Toluene
Xylenes
U.S. EPA-Method 8010
Bromodichloromethane
Bromoforo
Bromomethane
Carbon Tetrachloride
Chlorobenzene
Chloroethane
2-Chloroethylvinyl ether
Chloroform
Chloromethane
Dibromochlororoethane
1,2-Dichlorobenzene
1,3-Dichlorobenzene
1,4-Dichlorobenzene
Dichlorodifluoromethane
1,1-Dichloroethane
1,2-Dichloroethane
1,1-Dichloroethene
tranc-1,1-Dichloroethene
1,2-Dichloropropane
cis-l,3-Dichloropropene
trans-1,3-Dichloropropene
1,1,2,2-Tetrachloroethane
Tetrachloroethane
1,1,1-Trichloroethane
1,1,2-Trichloroethane
Trichloroethene
Trichlorofluoromethane
Vinyl chlorida
M«thyltn« chloride
32683.5
Pretreatment
Lc
ND 50
ND 1
ND 1
ND 1
ND 1
ND 50
ND 50
ND 50
ND 2
ND 2.
ND 2
ND 2
ND 2
ND 2
ND 2
ND 2
ND 2
ND 2
ND 2
ND 2
ND 2
ND 2
ND 2
ND 2
ND 2
ND 2
ND 2
ND 2
ND 2
ND 2
ND 2
ND 2
icati
7.3
15
8.3
150
32683.5
Post-treatment
NO 1.
ND 0.02
NO 0.02
ND 0.02
ND 1.
ND 1.
ND 1.
9.7
ND 0.02
ND 0.02
ND 0.02
ND 0.02
ND 0.02
ND 0.02
ND 0.02
32678.5
Pretreatroent
32678.1
Post-treati
Location 10
ND 1.
ND 0.02
7.6
ND 0.02
ND 0.02
20
1
34
ND 0.02
ND 0.02
ND 0.02
ND 0.02
ND 0.02
ND 0.02
0.02
ND
ND
ND
0.43
0.02
0.02
7.6
ND 0.02
ND 0.02
ND 0.02
MD 0.02
ND 0.02
ND 0.02
ND 0.02
ND 0.02
ND 0.02
ND 0.02
ND 0.02
ND 0.02
ND 0.02
3.6
7.9
ND 0.02
ND 0.02
ND 1.
ND o.o:
ND o.o;
ND o.o;
ND 1.
ND 1.
ND 1.
ND o.o;
ND o.o;
ND o.c;
ND 0.02
ND o.o;
ND o.o;
ND o.o;
Note: All values shown are in mg/kg.
ND x indicates that compound was not detected at a concentration in excess of
x mg/kg. Where no value is reported for a particular compound, that compound was
not analyzed in post-treatment soil samples.
-------
E-6
COMPARISON OF PRETREATMENT AND POST-TREATMENT SOIL CHARACTERIZATION
LOW TEMPERATURE THERMAL AERATION PROCESS
MCKIN SUPERFUND SITE
GRAY, MAINE
(Continued)
SAMPLE I.D. 32673.5 32673.5 32668.5 3266
Type Pretreatment Post-treatment Pretreatroent Post-tr«
U.S. EPA Method 8020 Location 11 Location 12
Benzene ND 50 NO 1. ND 50 ND
l.Chlorobenzene ND 1 ND 1
1,2-Dichlorobenzene 22 ND 0.02 ND 1 ND 0
1,3-Dichlorobenzene ND 1 ND 0.02 ND 1 ND 0
1,4-Dichlorobenzene ND1 ND 0.02 ND 1 ND 0
Ethylbenzene ND 50 ND 1. ND 50 ND
Toluene ND 50 ND 1. ND 50 ND
Xylenes 62 ND 1. ND 50 ND
U.S. EPA Method 8010
Bromodichloromethane ND 1 ND 2
Brocnof orm ND 1 ND 2
Bromomethane ND 1 ND 2
Carbon Tetrachloride ND 1 ND 2
Chlorobenzene ND 1 ND 2
Chloroethane ND 1 ND 2
2-Chloroethylvinyl ether ND 1 ND 2
Chloroform ND 1 30
Chloromethane ND 1 ND 2
Dibromochloromethane ND 1 ND 2
1,2-Dichlorobenzene 22 ND 0.02 15 ND
1,3-Dichlorobenzene ND 1 ND 0.02 ND 2 ND
1,4-Dichlorobenzene ND 1 ND 0.02 ND 2 ND
Dichlorodifluoromethane ND 1 ND 2
l,l-Dichloro«than« ND 1 ND 2
l,2-Dichloro«than« ND 1 ND 2
l,l-Dichloro«th«n« ND 1 ND 2
tran«-l.l-Dichloro«th«n« ND 1 ND 0.02 ND 2 ND
l,2-Dichloroprop«n« ND 1 ND 2
cis-l,3-Dichloroprop«n* ND 1 ND 2
tran«-1.3-Dichloroprop«n« ND 1 ND 2
l,1.2,2-T«trachloro«than« ND 1 ND 2
T«trachloro«thane 2.7 ND 0.02 6 ND
l,l,l-Trichloro»th«n« 0.14 ND 0.02 2.9 ND
1,1,2-Trichloroethane ND 1 ND 2
Trichloroethene 34 ND 0.02 314 ND
Trichlorofluoromethane ND 1 ND 2
Vinyl chloride ND 1 ND 2
Methylene chloride ND 1 IS
Note: All values shown are in mg/kg.
ND x indicates that compound was not detected at a concentration in excess of
x mg/kg. Where no value is reported for a particular compound, that compound
was not analyzed in post-treatment soil samples.
-------
APPENDIX F
COMPARISON OF PRETREATMENT AND
POST-TREATMENT SOIL CHARACTERIZATION -
PETROLEUM AREA SOILS
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-------
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-------
F-2
COMPARISON OF PRETREATMENT AND POST-TREATMENT SOIL CHARACTERIZATION
PETROLEUM AREA SOILS REMEDIATION
LOW TEMPERATURE THERMAL AERATION PROCESS
MCKIN SUPERFUND SITE
GRAY, MAINZ
(Continued)
SAMPLE I.D.
Typ*
Ac«naphth«n«
2,6-Dinitroph«nol
4-Nitroph«nol
2,4-Dinitrotolu«n«
Diethylphthalat*
4-Chloroph«nyl-ph«nyl«th«r
Fluor«n«
B*nzidina
4,6-Dinitro-2-M«thylphenol
N-Nitrocodiphvnylamine
4-Bromophenyl-ph«nylath«r
H«xachlorob«nz«n«
P«ntachloroph«nol
Phenanthran*
Anthracene
Di-N-Butylphthalate
Fluoranthen*
Pyrene
Butylbenzylphthalate
3,3'-Dichlorobenzidine
B*nzo(a)Anthracene
bi«-(2-Ethylhexyl) Phthalate
Chrytene
Di-N-Octyl Phthalate
B«nzo < b)Fluoranthene
Benzo(k)Fluoranthene
Benzo(a)Pyrene
Indendo(l,2,3-cd)Pyrene
Dibenzo(a,h)Anthracene
Benzo(g, h, i)Peryl«n«
Total Extractabl* Hydrocarbon*
323A
Pr>tr«atin«nt
KD 0.330
ND 0.330
ND 0.330
ND 0.330
ND 0.330
ND 0.330
ND 0.330
ND 0.330
ND 0.330
ND 0.330
ND 0.330
ND 0.330
ND 0.330
0.850
0.790
ND 0.330
0.330
ND 0.330
ND 0.330
ND 0.660
ND 0.330
ND 0.330
ND 0.330
ND 0.330
ND 0.330
ND 0.330
ND 0.330
ND 0.330
ND 0.330
ND 0.330
323B
Po«t-tr«atro«nt
ND 0.330
ND 1.650
ND 0.330
ND 0.330
ND 0.330
ND 0.330
ND 0.330
ND 0.330
ND 1.650
ND 0.330
ND 0.330
ND 0.330
ND 1.650
0.630
ND 0.330
ND 0.330
ND 0.330
ND 0.330
ND 0.330
ND 0.660
ND 0.330
ND 0.330
ND 0.330
ND 0.330
ND 0.330
ND 0.330
ND 0.330
ND 0.330
ND 0.330
ND 0.330
329A
Pr«tr««tm«nt
ND 0.330
ND 0.330
ND 0.330
ND 0.330
ND 0.330
ND 0.330
ND 0.330
ND 0.330
ND 0.330
ND 0.330
ND 0.330
ND 0.330
ND 0.330
1.200
1.200
ND 0.330
0.340
ND 0.330
ND 0.330
ND 0.660
ND 0.330
ND 0.330
ND 0.330
ND 0.330
ND 0.330
ND 0.330
ND 0.330
ND 0.330
ND 0.330
ND 0.330
329
Post-tra
ND 0.33
ND 1.65
ND 0.33
ND 0.33
ND 0.33
ND 0.33
ND 0.33
ND 0.33
ND 1.65
ND 0.33i
ND 0.33i
ND 0.33i
ND 1.651
O.Sll
ND 0.33<
ND 0.33(
ND 0.331
ND 0.33(
ND 0.33C
ND 0.66C
ND 0.33C
ND 0.33(
ND 0.33C
ND 0.33C
ND 0.33C
ND 0.33C
ND 0.33C
ND 0.33C
ND 0.33C
ND 0.33C
1800
690
1600
70C
Not*: All valuas shown arc in mg/kg.
ND x indicate* that compound was not d«t«ct*4 at a concentration in axcasc of
x mg/kg.
-------
F-3
COMPARISON OF PRETREATMENT AND POST-TREATMENT SOIL CHARACTERIZATION
PETROLEUM AREA SOILS REMEDIATION «"«*
LOW TEMPERATURE THERMAL AERATION PROCESS
MCKIN SUPERFUND SITE
GRAY, MAINE
SAMPLE I.D. 326A 326B
TYP* Pratraataant Poat-traatmant
U.S. EPA Method 8020 Location 15
B«nzana ND 0.2 ND 0.2
Chlorobanzana ND 0.2 ND 0.2
1,2-Dichlorobanzana 1.5 ND 0.2
1,3-Dichlorobanzana ND 0.2 ND o!2
1,4-Dichlorobanzana ND 0.2 ND 0^2
Ethylbanzana 1.3 ND o!2
Toluana 0.2 ND 0.2
Xyl«nas 3.3 ND 0.2
U.S. EPA Mathod 8270
N-Nitroaodiathylamina ND 0.330 ND 0.330
phtno1 ND 0.330 ND 0.330
bit <-2-Chloro«thyl) Eth«r ND 0.330 ND 0.330
2-Chloroph«nol ND 0.330 ND 0.330
l,3-Dichlorob«nz«n« ND 0.330 ND 0.330
l,4-Dichlorob«nz«n« ND 0.330 ND 0.330
l,2-Dichlorob«nz«n« 0.710 ND 0.330
bis (2-chloroi«opropyl) Eth«r ND 0.330 ND 0.330
N-Nitroto-Di-Propylamina ND 0.330 ND 0.330
H«xachloroathan« ND 0.330 ND 0.330
Nitrobanzana ND 0.330 ND 0.330
iBophorona Q.450 ND 0.330
2-Nitrophanol ND 0.330 ND 0.330
2,4-Dioathylphanol ND 0.330 ND 0.330
bi« (-2-Chloroathoxy) Nathana ND 0.330 ND 0.330
2,4-Dichlorophanol ND 0.330 ND 0.330
1,2,4-Trichlorobanzana ND 0.330 ND 0.330
Naphthalana ND 0.330 ND 0.330
Haxachlorobutadiana ND 0.330 ND 0.330
4-Chloro-3-Mathylphanol ND 0.330 ND 0.330
Haxaehlorocyclopantadiana ND 0.330 ND 0.330
2,4,6-Trichlorophanol ND 0.330 ND 0.330
2-Chloronaphthalana ND 0.330 ND 0.330
Dimathyl Phthalata ND 0.330 ND 0.330
Acanaphthylana ND 0.330 ND 0.330
2,6-Dinitrotoluana ND 0.330 ND 0.330
-------
F-4
COMPARISON OF PRETREATMENT AND POST-TREATMENT SOIL CHARACTERIZATIOM
PETROLEUM AREA SOILS REMEDIATION n*rm^"UZATION
LOW TEMPERATURE THERMAL AERATION PROCESS
MCKIN SUPERFUND SITE
GRAY, MAINE
(Continued)
SAMPLE I.D.
Typa
Acanaphthana
2,4-Dinitrophanol
4-Nitrophanol
2,4-Dinitrotoluana
Diathylphthalata
4-Chlorophanyl-phanylathar
Fluorana
Banzidina
4,6-Dinitro-2-Mathylphanol
N-Nitroaodiphanylamina
4-Brcraophanyl-phanylathar
Haxachlorobanzana
Pantachlorophanol
Phananthrana
Anthracana
Di-N-Butylphthalata
Fluoranthana
Pyrana
Butylbanzylphthalata
3,3' -Dichlorobanzidina
Banzo(a)Anthracana
bii-(2-Ethylhaxyl) Phthalata
Chrycana
Di-N-Octyl Phthalata
Banzo(b)Fluoranthana
Banzo(k)Fluoranthana
Banzo(a)Pyrana
Indando(i,2,3-cd)Pyrana
Dibaiuo(a,h)Anthracana
Banzo(g,h,i)P«ryUn«
326A
Pratraatmant
NO 0.330
ND 0.330
NO 0.330
ND 0.330
ND 0.330
ND 0.330
ND 0.330
ND 0.330
ND 0.330
ND 0.330
ND 0.330
ND 0.330
ND 0.330
1.100
0.810
ND 0.330
0.800
ND 0.330
0.44O
ND 0.660
ND 0.330
ND 0.330
ND 0.330
ND 0.330
ND 0.330
ND 0.330
ND 0.330
ND 0.330
ND 0.330
ND 0.330
326B
Poit-traatnant
ND 0.330
ND 1.650
ND 0.330
ND 0.330
ND 0.330
ND 0.330
ND 0.330
ND 0.330
ND 1.650
ND 0.330
ND 0.330
ND 0.330
ND 1.650
0.540
ND 0.330
ND 0.330
ND 0.330
ND 0.330
ND 0.330
ND 0.660
ND 0.330
ND 0.330
ND 0.330
ND 0.330
ND 0.330
ND 0.330
ND 0.330
ND 0.330
ND 0.330
ND 0.330
Nota: All valuat shown ara in mg/kg.
ND x indieataa that compound was not datactad at a
concantration in axcaaa of x mg/kg.
-------
APPENDIX G
DECONTAMINATION CERTIFICATION
CanonieEnvironmenta!
-------
G-l
APPENDIX G
DECONTAMINATION CERTIFICATION
The construction and process equipment was decontaminated using a hot water
pressure cleaner to remove all visible surface soil and surface
contamination.
The criteria for decontamination certification are:
1. Absence of a visual identification of foreign substances, colors,
or films;
2. Absence of any sources of organic vapor evolution, as monitored by
a Century Organic Vapor Analyzer.
I certify that the decontamination was completed in accordance with the
Closure Action Work Plan of October, 1985.
4' SU I rN ' I
c^J.»w.rn>v^ ^ yfflUu^Qfr^
Timothy/./ Harrington, P/E.
State ofv>(aibe Professional Engineer #5282
CanonieEnvironmentai
-------
APPENDIX H
MANIFEST FORMS -
TRANSPORTATION AND DISPOSAL OF
WASTE MATERIALS
CanonieEnvironmentai
-------
4O-14-1 \4
-------
48-14-1 (4/85)
Please print or type.
STATE OF NEW YORK
DEPARTMENT OF ENVIRONMENTAL CONSERVATION H-2
DIVISION OF SOLID AND HAZARDOUS WASTE
HAZARDOUS WASTE MANIFEST
P.O. Box 12820, Albany, New York 12212 Form Approved. OMB NO. 2000-0404 expires 731^6
UNIFORM HAZARDOUS
WASTE MANIFEST
. Generator's US EPA No.
Manifest
2. Page 1
Information in the shaded are;
is not required by Federal La*
3 Generator's Name and Mailing Address
)
C V I AJ
"5 /TE-
4. Generator's Phone (
S. Transporter 1 (Company Name)
6. US EPA ID Number
7. Transporter 2 (Company Name)
8. US EPA ID Number
! I ' ! I I I
r. TI
9. Designated Facility Name and Siti Address
10. US EPA ID Number
H V fl o f9 8 5,4
H,
S23T
T3. Speclat Mananng Instructtoru
11. US DOT Description (Including Proper Shipping Name, Hazard Class and ID Number)
16. GENERATOR'S CERTIFICATION: I hereby declare mat the content! of thu consignment are fully end accurately described above by prooer iruppmg name ana .
classified, packed, mamed and labeled, and are in all reapects in proper condition for transport by fiignway according to applicable international and national governmi
regulations and state laws and regulation*.
Unless I am a small quanttty generator «mo fieeeeen exempted by statute or regulation from me duty to make a waste minimization certification under Section 3002 ibi
RCRA. I also certify met I neve a erogrem (ej eeM9B reduce volume and toiicity ol««s*e.generated to trte degree i nave determined to be economically practicable and i ng
selected the metnod o( treatment storage, or disposal currently available to me X"Kn l«nimiies the prejf/it an^TVure tjyeat to numan neaitn and the environment
M BELL
Printed/Typed
Signati
MO, Oa
j /
17. Transporter i (Acknowledgefnent of Bece4pt of Materials)
Printed/Typed
Signature
Mo. Day v
18 Transporter 2 (Acknowledgement or Receipt of Materials)
Printed/Typed Name
Signature
Mo. Day Y
I I I
19. Discrepancy Indication Space
20 Facility Owner or Operator: Certification of receipt of hazardous materials covered by this manifest except as noted in item 19
EPA FOIW ITOO-M (He*. 44s> Prev.ous edition is obsolete. COPY 3—Generator—mailed by TSD facility
-------
46-14-1 (4/85)
e
Please print or type.
STATE OF NEW YORK
DEPARTMENT OF ENVIRONMENTAL CONSERVATION "~ 3
DIVISION OF SOLID AND HAZARDOUS WASTE
HAZARDOUS WASTE MANIFEST
P.O. Box 12820, Albany, New York 12212 Form Approved. OMB NO. 20004404 Expires 7.31-61
i
«
a
•
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c
o
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Jl
i
UNIFORM HAZARDOUS
WASTE MANIFEST
Information in the shaded art
ia not required by Federal La\
3. Generator's Name and Mailing Address
5 Transporter 1 (Company. Name) \
7. Transporter 2 (Company Name)
9. Designated Facility Name and Site Address
/v y Ufa? IN .ID .ortftft 3M,7
fJ t
11. US DOT Description (Including Proper Shipping Name, Hazard Clasa and ID Number)
15 Special Handling Instructions and Additional Informa
16 GENERATOR'S CERTIFICATION: I Hereby declare trial me contents of ttil* coniignrnent *re fully and eecuretely deteribed atfeve by proper ttiipping nlm« and i
classified. pacKM. marked end leeeied, and we in aH reepeet* in proper condition lor transport by ntgftway according to applicable international end national governmi
regulations and (tale laws end regulations.
Unices I am a smell Quantity muetaUK •«» (Mteean eiempted By statute or regulation from the duty to make a oasts minimization certification under Section 3002 101
RCPA. i also certify mat t neve a program In aSe to reduce volume end toxicity of waste oiQerated to the degree I have determined to be economically practicable and I ni
selected the method of treatment storage, or alepeeal currently available lo me wfticn^mTrnVe* the present and future tMfftt to huaapn health end the environment
— i — *• • t- y - j~rf^"~~TP^~~iaTrJTr' ""' .. ' ~"~' —
17
Transporter ^ (Ackriowtwdgefnent of HsKelpt of Materials)
Printed/Typed N
Mo. Day
18 Transporter 2 (Acknowledgement or Receipt of Materials)
Printed/Typed Name
Signature
Mo. Day Y<
I I L_
19. Discrepancy Indication Space
20. Facility Owner or Operator Certification of receipt of hazardous materials covered
by tnn m
lanifeat except as noted in item 19
d in i
Printed;
Name
Signa
EPA Forni «70o M («e». 446) Previoua edition is obsolete COPY 3—Generator—mailed by TSD facility
-------
48-14-1 (4/85)
e
Please print or type.
STATE OF NEW YORK
DEPARTMENT OF ENVIRONMENTAL CONSERVATION
DIVISION OF SOLID AND HAZARDOUS WASTE
H-4
HAZARDOUS WASTE MANIFEST
P.O. Box 12820, Albany, New York 12212 Form Approved. OMB NO 20000404 e»Pire. 7.31 M
I 1. Generator's US EPA No. ~Manifest
hep a e o i j&tf 0 i? gtoggatt
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UNIFORM HAZARDOUS
WASTE MANIFEST
2. Pag..,
Information in the shaded areas
Is not required by Federal Law.
3. GeneratorNam. and Mailing Addr...
4. Generator's Phone ( )
5. Transporter 1 (Company Name)
7. Transporter 2 (Company Name)
9. Designated Facility Name and Site Address >
10. US EPA ID Number
11. US DOT Description (Including Proper Shipping Name. Hazard Claas and ID Number)
16 GENERATOR'S CERTIFICATION: I rwraey oaclara that th« contanta of tnia conaignmant am fully and accurately described above oy proper shipping name ana ar
classified, packed, manted and labeled, and an in all respects In proper condition for transpon by highway according to applicable international and national governmer
regulations and state law* and regulation*.
Unless i am a small quantity generator «no Me*teen aiempted by statute or regulation from in* duty to make a wast* minimization certification under Section 3002 Di c
RCRA, i also certify mat I have a program M ottoe to reduce volume and toxicity of «w*1l generated to the degree I iiam determined to be economically oracticafiia ana i nav
selected the metfjod of treatment, storages* *Je»uasl currently available to me »fKp /inimiies the present and XjtuYa threat Jt human nealtn and the environment
W&u.
Printed/Typed Name
Slgnati
Mo. Day
,1 I to
17 Transporter 1 (Acknowledgement of Receipt of Materials)
Printed/Typed Name
^^x/*
18. Transporter 2 (Acknowledgement of
Signature
iipt of Materials)
Mo. Day Ye
Printed/Typed Name
Mo Day Ye
II I
19. Discrepancy Indication Space
20. Facility Owner or Operator: Certification of receipt of hazardous materials covered by this manifest except as noted in item 19
Printed/Typed Name
Signature
Mo Day
EPA Fomi »no-22 (Rev. 448) Previous edition is obsolete COPY 3—Generator—mailvd by *so facility
-------
22oc CHURCHILL ROAD SPRINGFIELD ILLINOIS 62706 121?) 782-6761
if arm designs for use on elite '12-pitcfu typewriter i EPA FOfTTI 8700-22 (3-84)
H-5
:L532-0«'0
LDC 52 3 8'
Form Approved OMB No 200O-Q404 Exoires ~-3M
UNIFORM HAZARDOUS
WASTE MANIFEST
information -n me snaoeo areas .5
required By Federal law But is 'ecui
by Illinois law
Illinois Manifest Document Number
3 Generators Name and Mailing Address J—
4 Generator's Phone (
<&E/W..ME CX/Qg?
5 Transporter 1 Company Name
rsmportef s Phoni
US EPA ID Number
7 Transporter 2 Company Name
10 US EPA ID Number
9 Designated Facility Name andSite Address
11 US DOT Description (Including Proper Shipping Name. Hazard Class, and ID Number)
12. Containers
No.
o.
d.
A AS
Above.
WUtfPfD tu
HawdlingC«
in Ittmru
1 = Gallorw
•••0' •" :CI
tor Wsatee Listed
2 = Cubic Yards
15 Special Handling instructions and Additional Information
i A^Tt
PM7/2- i
16 afWDMTOMt CERTIFICATION: I hereby declare that the contents of this consignment are fully and accurately
proper snipping name and are classified, packed, marked and labeled, and are in all respects in proper conMMfl
highway according to applicable international and national government regulations, and Illinois regulations.
Unless I am a small quantity generator who hat been exempted by statute or regulation from me duty to make a waste minimization certification under Sectu
3002(b) of RCRA i also certify that I have a program m place to reduce the volume and toxicity of watte generated to the degree i have determined to
economically practicable and I have selected the method of treatment, storage, or^iieaoeal currently availabw to me which minimizes the present ana 'uto
threat to human health and the environment f^ } /} I Date
Pn
yped Name
Signalu
Monrn Day
7 Transporter 1 Acknowledgement of Receipt of Materials
^^^^^^^^_^^^^^^HH«^K^^V^^BIlMIBeillM^llllHHHVaiMieMIIII>M«HI^^^H^^H
Dale
Printed/Typed Name)
Signature
Monrn Day
8 Transporter 2 Acknowledgement of Receipt of Materials
Date
Printed/Typed Name
Signature
Month Day
19 Discrepancy indication Space ^^^ J? C^OUT^i OM^JiO^\ &&**- WsnU*AS £**m fCCCS
9OCO^L. ^otvtx -&vuo>*-. -&uLL* /~9-87 >(i2c*^vc-&J2jLrv*jLi-
20 Facility Owner or Operator Certification of receipt ot hazardous materials covered by this manifest except as noted in item 19
3ate
Printed* Typed Name
IN ILLINOIS 217 782-3637
Signature.
Monrn Day
O' J '-"-'' jcN'.< '-'.C -"LI
OUTSIDE ILLINOIS 800 424-8802 or 202
DISTRIBUTION PART -' GENERATOR PART^IEPA PART - 3 FACILITY PART -4TRANSPORTER PART-SIEPA PART-6GENERATOR
°E i •' OCNCHATOM COTr - PAKT i. DO NOT MMOVt »*Mt 1 mOM SfT UHTK COMMJETIO.
-• -0«'»IO' =' -*nt -c ••c»« S2« OOC 3»' tl. ;* • o-«l.o« «»i»*Cil-o« o' Ift't n»OWit-<3n Ti»y 'Mutt n t '.n» jO to $90000 Of fliv 0' -toW«" WO -mc«'>O«w»«W up '0 5 y««n) T»»tt 'Ortw "w 0**** lOC'O'tc 3. -•
". t"W
-------
i.v. ro.-iT rrr "?43-84>C
- - - *». t.6-
Form AOOTCTV^ OUS NO*MOO-0«V«'E W»
I UHIFORM HAZARDOUS
V/ASTE MAN'IFSST
. Ge-v-atcrs US EPA .0
I//1£D~7£C~5^
No „
- Q7&| P
vtamiest
2. Page 1
of /
inhxmoon in trta sruoed area* « n
required By Federal law. but • requi«
by uinoa H». •%. -.-
A. Illinois Manifest Oocumant
'
4 Generator's Phone
B.Illinois "'
Generator's
ID _•- :
5 Transcorter 1 Company Name
6.
US EPA ID Number
C.Illinois Transporter't
1 Transporter 2 Company Nam'e
US EPA ID Number
E.lllinois Tramporter'a
9 Designated Facility \arre anr; Si'.e Aiiress
10
US EPA ID Number
i;-K)0
11 US DOT Desc.''pT;on ', .rciuaing Proper Shipping Ai^me. Hazara Class, antf /O NumOtr)
Ctur
b.
K. Handling Cod« tor Waste* Liited.Abave ~.
»n Item §14 ; - ** ^ JiuJStT^ -
-1= Gallons ..^ 2==CubteYar(
"
;nt3r.-;ation
;irv~'.r CiT)CN: : n- 202.
f=" " ' •. P.I.-.T . . c:-.£= -.TC= PART.;IE"< PART. 3 FACILITY PART . 4 TBAN£^O*TCT
COPT -
• OO SOT BjUOvt t»>HT t
-------
H-7
HAZARDOUS WASTE MANIFEST
(As RiMMrad By The Alabama Department of Environmental Management)
MMM prim or type. fftrm
i OMff Ma JOOff-fffOf. fxaim 7-31 •*
WASTE MANIFEST
!• not required by Federal
4. Generator's Phone (
CHEMICAL WASTE MANAGEMENT. INC.
Emells Facility
Alabama Hi^io«y 17 at Mila Marktr 163
Em«ll«, Alabwna 35459
0, 0,0,6,2! 2,4,6|4
12. Comaker*
No. Type
11. US DOT Oeacnpnon///Mludvv Propar Stuping N*nu. Huirt Clut*. »nd ID Mun*ar*
CWM Profile Number
CWM Profile Number
CWM Profile Number
CWM Profile Number
centenu or trn» coniignment are fuHy end
end libeled, end are m eH reepeea m proper
regulation*.
proper *rtippine>
aooordinQ to
Unleee I am •
under Section
have
lejn tempted by patute or re*iletton f
I M«b a prfltrkm w ptaee'to reduce the
of weete generated to the degree
currently aveileMo to me which
endtheenvirooiT
Men0> Oer ?*
I I I I I
-------
H-8
HAZARDOUS WASTE MANIFEST
(A» Required By The Alabama Department of Environmental Management)
Emm. »*M
Heaae prim or type.
E40KXHj£
UNIFORM HA
nfermaoen m the artaded araaa
i» not required by Federal
low.
WASTE MANJEE8T
4. Generator s Phone (
7. iranaporter 2 Comp«ny PMme
CHEMICAL WASTE MANAGEMENT. INC.
Emelle Facility
Alabwna Hiotiw*y 17 at Mil* Marker 163
Emelle, Alabama 35459
CWM Profile Number -y-/ //5^
CWM Profile Number
CWM Profile Number
CWM Profile Number
16 GENERATOR**
proper shipping
according to
It I am a large
economically pr
future threat toJiwnM
"f ? • . ••• ' .' -..V
«.! • I —
tn» contenii 01 mis consignment are tuiiy and accurately deacnoed above by
. and labeled, and are in all respects in proper condition for transport by highway
nment regulations j ^
proo/am m place to reduce the volume and toncily ol waste rjenerated to the degree I have determined to be
acticable method ol treatment storage, or disposal currently available to me which minimnes the present and
.QM. i< I am a small quantity generator, I nave made a good lailh effort to minimize my waste generation and select
fx) lh*' ' can afford
/ ;
afford
Signature
Month Oey
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17.T
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Signatura '
/ , . / "'
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MOMT) Day Yi
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eiura .
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19 On
r Indtcatien Spi
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20.FacHrry Owner or Operator CaraftcaMn af
Printed/Typed Nama
o» hatardoua matanala. covwad by trva manrfaa
I Signature
m Nam 19
Month (Jay Y
I I 1 ! I
-------
H-9
HAZARDOUS WASTE MANIFEST
(Aa Btjqutoad By The Alabama Department of Environmental Management)
f-lease print or type.
OMB MD. 2060-OOW Sores 9-30+
UNIFORM HAZAH
WASTE MA
ia not required by Fedaral
>-i< .' •
Addrao*
CHEMICAL WASTE MANAGEMENT. INC.
Emelli Ftcility
Alabama Highway 17 at Mile Marker 163
Emelle. AUbame 35459
• A, LI Q 0, 0,0,8,2, 2
16 GENERATOR'S
proper shipping
according to
if I am a large
economically pr
future threat to human
me contents ot this consignment are lolly and accurately described above by
and labeled, and are m all respects m proper condition for transport by highway
nmem regulations
program m place 10 reduce the volume and toxicity of waste generated to the degree I have determined to Be
racticable method of treatment, storage, or disposal currently available to me which mmimnes the oresent and
. if I am a small quantity genernior. I nave made a good faith effort to minimize my waste generation and select
and that I can afford
i afford
SignatureZT
Month Oar
T
ft
A
N
S
•
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T
ft
17T
1
Prirnad/Tvpad Nama
ILL ,-
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Sionatura
month Day Y*
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187f
dgamam of
tfaaf A4a^i^^*B^Bi
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19.DiacrapancY Indication Spaca
V
20Ftaiitv Owmcr or Operator Coriffteation at rocMpi of h.uiraou« mmorula oovorod by the* manrfMt
as noead in Ham 19
•Vimad/Typad Kama
Signature
Afomn 0*i
-------
H-10
HAZARDOUS WASTE MANIFEST
(As Required By The Alabama Department of Environmental Management)
rtcaae print or typo.
Form Approved. OMB No 206CMWW Enma 9-30-ai
UNIFORM HAZARDOUS
WASTE MANIFEST
1. generator t US EPA IP No. > ^
"'
Information in the shaded area*
it not required by Fedora)
—T—I V. >
t t-A/*
4. Generator's Phono (
)
s. iraneporter i company Name
: /. • c.
T.
transporter 2 Compony Nomo
9. ueaignated Facility Name and Silo Addrees"
CHEMICAL WASTE MANAGEMENT. INC.
Email* Facility
Alabama Highway 17 at Mile Marker 163
Email*, Alabama 35459
11. US DOT Deacnpnon (Including Prop* Shipping Mama. Huurd C/au. a/rt ID Humbert
C.
CWM Profile Number
CWM Profile Number
CWM Profile Number
CWM Profile Number
IrtorMation
16
GENERATOR'S C
proper shipping n
according to apphcalUa
that tne contents ot tnu consignment are tuliy and acccxately described above by
tad. and labeled, and are in all respects in proper condition lor transport by hignwav
nment regulations
m am a large quantity
economically Ofi
future threat 10 human
ine
UMUMuma a program m place to reduce the volume and toiicitv ot waste generated to tne degree I have determined 10 Be
the practicable method of treatment storage, or disposal currently available to me which mimmites tne present and
. it I am a small quantity generator. I have madea good lann effort to minimise my waste generation and select
10 me and that I can altord
ELL
altord
Signature
Month Oar Y*>
K I. I; I. I I
T
M
A
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•
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T
I
17Ti
Primad/Typod Name
Sianatwra,
Month Day Y»i
\ i, I A.- I • I
2 Xeki
Sigoatunj-
Month Off Yi,
II I/1. Y \
19.0in
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20 Facility Owner or Oparator Canmcation of racaaj* of haardoua matariala covorad by tnia mamtaai
aa nowd in ham 19
Pnmad/Typad Name
Signature
Month Otr ft
[ ' I ' 1
-------
H-ll
HAZARDOUS WASTE MANIFEST
(At HaquJnirl By The Alabama Department of Environmental Management)
l-leeae pnnt or type.
UNIFORM
WASTE
4. Generator's Phone (
US EPA K> Number
9. Doennatod Facility Name and Sit*
CHEMICAL WASTE MANAGEMENT. INC.
Email* Facility
Alabama Highway 17 at Mil* Marker 163
Email*. Alabama 35459
| A, L| Q 0, 0,0, 6,2, 2
11. US OCKQlBnptHinllncludHttPrcv* Stopping Mum*
.•«.<•/ ,;
CWM Profile Number
GENERATOR:*
proper sh
according to
H I am a large.
•conomically
future threat
in* contents of this eomignmeni are fully and accurately described above-Ay
and labeled, and are m all respect* in proper condition for transport by Highway
it regulations
program in place to reduce the volume and toiicitv ol waste generated to the degree I have determined to be
acncaWe method of trealment. storage, or disposal currently available to me which mmimues the present and
if I am a small quantity generator. I have mad* a good faith effort to minimise my waste generation and select
can afford
/
Day Yi
' \'C fc
T
N
A
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O
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Oar
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2 *rtrne»led9*meni of
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Oay Y,
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19.0tacrep*ncy Indication Space
20 Feolriy Ownef or
CtttlfiOMfl Of
at hanrdou* metenele
t«M ftaaM
-------
H-12
HAZARDOUS WASTE MANIFEST
By The Alabama Department of Environmental Management)
• US 6PA W NO. ^
is net require* ,v Federal
US EPA IB Number
CHEMICAL WASTE MANAGEMENT. INC.
Emelle Facility
Alabama Highway 17 at Mile Marker 163
Emelle, Alabama 35459
• A, L, 0, 0, 0,0,6,2, 2
CWM Profile Number
16 GENERA
proper
according to
if I am a lar
economically
future threat
irteeentenu ot tmi consignment are fully and accurately described above by
I. and labeMd. and are m all respects in proper condition tor transport by nignwav
regulations
am in place to reduce the volume and toiicitv ol wawa generated to the degree I have determined 10 oe
icaMe method ol treaiment. storage, or disposal currently available to me which minimaes the present and
it I am a small Quantity generator. I have made a good lanh effort to minimise my waste generation and select-
lean atfi
/ I
A/
H.T
2 AeknowlMki
Oey Ytt
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Oar f*
I I I I I
zO.Faaltty OVMWT or Operator CeraAeMon «f
rWedTTyped B5ST
Monert Oey
I I I I
-------
H-131
HAZARDOUS WASTE MANIFEST
By The Alabama Oepertment of Environmental Management)
not required by Federal
US EPA 10 Number
If I am a large)
economically
future threat
tne contents ot mis ce**a]nment.*r« rulry and accuraialy described above by
end labeled, and are in air respects m proper condition (or transport by highway
regulations
program m place to reduce the volume and teucity ot waste generated to tne degree I neve determined to be
acucable method of treatment storage, or disposal currently available to me which mimmnes the eresent and
if I am a small quantity generator. I have mad* a good lailh effoct to mmimiie my waste generation and select
that I can afford
Signature =~*~ ~T" Montr) Day Y
Oey
MaMr> Oay Y
«r*4 by
Month Oay
-------
H-14
HAZARDOUS WASTE MANIFEST
By The Alabama Department of Envkonm«nt«i
•""•—" — — —» •— "^ •••••••••laB oJTMV
i« not required by Federal
• r " w • * * •
r TEV-^C /.v^.
I <•- "'X ' «i.r '^4
- . f
4. Generator's Phone I
s! iraneporter 1 Company Name 6.
.
US EPA IO Number
7 Transporter 2 Compeny Name
EPA 10 Number
I I I I I I I
91 oatignateo haallty n»m» and
CHEMICAL WASTE MANAGEMENT. INC.
Emelle Facility
Alabama Highway 17 at Mile Marker 163
Emrtle, Alabama 35459
A, L| D| 0| 0|0|6|2| 2
11. US DOT Description rMc/udtof Proper Sniffing /Vame. Hmitrd Cltf*. vtd ID Munrittfl
CWM ProfHe Number C
CWM Profile Number
CWM Profile Number
CWM Profile Number
16 GEMCRAT
proper sn
according to
the contents ot rnis consignment are tally and* accurately descnood abov* by
and labeled, and are in all respects m proper condition Iw transport by nignwav
regulations
it I am a large
economically
future threat
ogram m place to reduce the volume and toxicitv ot waste generated to ine degree I nave determined to Be
awe method ol treatment, storage, or disposal currently available to me which minimizes the present and
m a small quantity generator. I have made a good laitn effort to mm imite my waste generation and saiect
that i can atlord
in» b»»t waste
Primed/Typed
Month Day Ytt
: \t"\J\ /I ' I
Oey Ytt
I I I I I I
1 S.Diacrapency Indicaoon Space
»•
A
C
1
I
T
y
20 facility Own** or Operator CortMeMon of retwpl of haordflua mMenoM ooverad ky «* meni
-------
H-15
HAZARDOUS WASTE MANIFEST
(As Required By The Alabama Department of Environmental Management)
Form *opro»ed. OMB No. aogfrprm Eipna 9-3041
TnwriSS!e«nr3!eT!eded™*reee"
is net required by Federel
tmi 11
UNIFORM
WASTE MANIFEST
4. Generator's Ptione (
US EPA 10 Number
9. Designated Facility Nam* and Site
CHEMICAL WASTE MANAGEMENT. INC.
Emelle Facility
Alabama Highway 17 at Mile Marker 163
Emelle, Alabama 35459
A, n 0, 0| 0|0,6|2| 2
11. US DOT Ottcn»tor> (Ine/uding freptr Stitpfing N»m». Hmtva Cl»t*. fo^ ID Mun^ffl
CWM Profile Number
CWM Profile Number
CWM Profile Number
16 GENERATORS
oroper shipping rvarae
according to
if i am a large quewMV
economically pr
future threat teh\ime*>
I the contents ot tms consignment are fully and accurately described above by
. and labeled, and are m all respects m proper condition for transport by highway
nment regulations
rprogram m place to reduce the volume and loudly of waste generated to the degree I have determined to be
acticable method ot treatment, storage, or disposal currently available to m* which minim.tes the present and
Off. if I am a small quantity generator. I have made a good faith effort to minimize my waste generation and select
Month Day
Signature
Momn Oay K
_L t- Ll'il
IMrrred/Typed rfimeT
Sigrwnn
Month Oay Yt,
I I I I I I
1 a.Diacrepency indtenion Spece
•
A
C
I
I
TO Facility Owner or Operator: Cemffcsnon of
Fnnted/Typed Neme
of haardou* rnetenaM cowered by Ihie manrfeei
1 v
Signetur*'
Month Oar X*
I i I
I I
-------
H-16
HAZARDOUS WASTE MANIFEST
(Aa Required By The Alabama Department of Environmental Management)
Mease print or type. Iftrm
Form Approved. OMB No 20SO-003B. Eipnt 9-304
ilrunlw riAetAmstHio |.:^7\T ;: 7- r /
WASTE MANIFEST . JMEROl QlOlOlOl /
ii not required by Federal
4. Generator's Phone (
a. transporter i company
irantponer i company iwiq*_ . . U
V/t.1 /*/'f ^^/'AT; ..i/ilil'nV
anaporter Z Company 'Name
9. MngnaMd Facility Name) and Site;
CHEMICAL WASTE MANAGEMENT, INC.
Emelle Facility
Alabama Highway 17 at Mile Marker 163
Emelle. Alabama 3
I A, L| D, 0, 0,0|6|2| 2
11. US DOT Description (Including Proper Stupptng Hum. Mturd C/au a/tf /O Number!
t6 GENERATON'S
proper snipping name 4
according to applicable i
at the contents ol thisconsignmem are tuny and accurately described above by
10. and labeled and are m all respects in proper condition lor transport by highway
irnment regulations
it i am a large quantity gejMajaar.1 certityHeM I rtfve a program in place to reduce the volume and tomcity ol waste generated to the degree I have determined to o»
economically practicebia*fleMtaUhav* tettojad (Impracticable method ol treatment,slorage. or disposal currently available to me which mimmxes the present and
future threat to human h*)*jM*ajAi>«h*)*nviro«MBam: OK. it I am a small quantity generator. I have mad* a good laith ellort to minimize my waste generation ano select
meftasi wame marmoaaMOl m*thod that is awailaM* Muna and that I can allord
17.Tranapenar 1 Ackno«r4*dg*m*nt of
sCtdJj m. '^OL
aKord
SionaMr* '
Month Oax Xei
Of MMeVMto
Prinwd/Typad Nam*
Month On y»i
I U.I/1 I I.
it.Tr«n*pomr I A<
PrtmadATypad Nam*
Sigoatur*
Month On
I
I
19.0racr*p*ncy Indjcmwn Spac*
20 Facility Owner or Operator Certification of
o< hasardeua rrujeanala aavatad by thai
m iMin 19
Prinwd/Typed Nam*
OTfVVT) 0*, 1 y*7»
Signature
Month On
1 I I ' I
-------
H-17
•lease print or typo. /form
HAZARDOUS WASTE MANIFEST
(As Required By The Alabama Department of Environmental Management)
I^rutftn»»ft12-filchltypuwrittf)fom Appiov*d. OMB No. XKHttM. Eiprae *.»-•«
UNIFORM HAZARDOUS
WASTE MANIFEST
\o\c\c io \O\l\L
4 Generator's Phone (
mniponw l Company Name
i i rensporter i company/ mam*
9! MsignatM Facility Name and Sit*
CHEMICAL WASTE MANAGEMENT. INC.
Emelle Facility
Alabama Higtiwav 17 at Mile Marker 163
Emelle, Alabama 35459
A, L, 0, 0, 0,0,612. 2 4. 61
11. US GOT Oiicri&ton {Including **»" StitpptngN»m*.HutraCI»u.»adU)Numb*rl
CWM Profile Number
CWM Profit* Number
CWM Profit* Number
CWM Profit* Numb*r
16 GENERATOR'S CEMTinG>%TIOtt'thei«sMMI*4feVD>*t in* contents ot this consignment are luliy and accurately described above by
proper snipping nam* Hid *n'Vir.
Month
I' \ ' I
Stgnatur*
Month
I I I
Y»t
I I
19.0i*erep*ncy Indieaiion Span
A
C
1
L
T
Y
Printed/Typed Nam*
Signature Month Cay Ytt
1 ' 1 ' 1 '
-------
H-18
HAZARDOUS WASTE MANIFEST
(As Required By The Alabama Department of Environmental Management)
•leas* prim or type, fftrm aajajnarfUr i«a an t**(12-p»eh) lypewnifarj
Form Approve*. OMB No. 208»oa>. Eiena 9-30-W
information in tna shaded are**
it net required by Fadaral
Generator's Phona (
..
ompany ame
US EPA 10 Number
CHEMICAL WASTE MANAGEMENT, INC.
Emelle Facility
Alabama Highway 17 at Mile Marker 163
Emelle, Alabama 35459
, L| 0, 0| 0, 0,6|2| 2
11 US DOT Deeeription llndudmg Prop* Shipping Nun*. Hunni DM* and ID Numbtr)
CWM Profile Number
CWM Profile Number
CWM Profile Number
CWM Profile Number
16
^^^^^^^ _^__ •"*' m* conl<" 'his consignment are tully and accurately described above by
proper shipping name aeVSMpMM. ffMB|B%Mrkad. and labeled, and are m all respects m proper condition lor transport by highway
according to ipphcsbta eSMJjH*^!^ •**Jaayia>^rnmeni regulations
it i am a large quantity gaealfilrrlWMifyMMMMaWa program m place to reduce the volume and toueity of waste generated to the degree I have determined to be
economically practicaMMNMkMfeawasaaietlJMnapracticable method of treatment storage or disposal currently available to me which mimmites the present and
future threat to rnjman haaMMaMwerwwej|*Mne O*l. if I am a small quantity generator. I have made a goed taith effort to minimize my waste generation and select
Month Oar
\r \: I /it'
I i
Primed/Typed NarneT
Signatura
It I
On re*
I I 'I
0 IB. Tr
H
of Ri
of Material*
Signatura
Moncn Oay fee
I I I ! I I
f
A
C
I
T
y
20.F*cilny Owner or Operator Certification of receipt of riaordou* matanal* covarad by true manrteai ««ex as noted m Hem. 19
PnntadyTypad Nam* Signature Month Oay Yn
| i | i | i
-------
H-19
HAZARDOUS WASTE MANIFEST
(As Required By The Alabama Department of Environmental Management)
Mease pnm or type. Iftrm
Form Approved. OMB No. 3060-OCCM Ex
UNIFORM HAZARDOUS
WASTE MANIFEST
» ua EI-M tw ran.
u-VjJC';r i.i
nformatkm in MM shaded areas
i* not required by Federal
' + ,< • - ,X
4. Generator's Phone (
D«wonat*d Facility Nam* and Sit* Addreea
CHEMICAL WASTE MANAGEMENT. INC.
Emelle Facility
Alabama HignvMy 17 at Mile Marker 163
Emelle, Alabama 35459
11.. US DOT DMeription flneludmg Prop* Shipping Mam*. Hutrd Cl***. »nd ID Humbvt
CWM Profile Number
CWM Profile Number
CWM Profile Number
CWM Profile Number
16 GENERATOR'S CM
proper shipping name
according to
if i am a large quantity
economically praeti
future threat tohurtiaej
irie
Vwt the contents ot this consignment are tuily and accurately described above by
I. and labeled, and are m all respects in-proper condition for transport by highway
nment regulations
a program in place to reduce the volume and loxicny of waste Generated to the degree I have determined 10 oe
practicable method of treatment, storage, or disposal currently available to me which mmim>(es the oreseni and
. if I am a small quantity generator. I have made a good faith effort to minimise my waste generation and select
nd that I can allorO
laflorO
Signature
Month Oar
'
Xe<
17 Transporter 1 Acknowtedgament of Naewpt of Minrnn
rnnted/Typed Name
Sionatura
Month On
I I I I I
IS.Tranaoomr 2 Acfcnowriedgament of MI
of Matanala
Signatura
Month Oey
I 1 1 1 I
19 Discrepancy Indieation Spaea
C
I
I
20 Faoiriy O«mar or Oparator Cartmcauon of racwpt of rwardoua maiariaW covwad by ttw manrfaat
M nowd in ttam 19.
Signatura
Month Oay Yt
I
I
I
-------
H-20
HAZARDOUS WASTE MANIFEST
(As fTanuirert By The Alabama Department of Environmental Management)
Hease prim or type. (firm
Porm Approved. OM8 Mo. 20504038. Eipn. 9-30-m
UNIFORM HAZAHBOUB
WASTE MANIFEST
ie net required by Federal
4. Generator's Pnone (
9. iranaponar 1company Name
ransporter 2 Company Name
9! Designated Facility Name and Site Addrees
CHEMICAL WASTE MANAGEMENT. INC.
Emelle Facility
Alabama Hi^iway 17 at Mile Marker 163
Emelle. Alabama 35459
• A, L| 0, 0, 0,0,6,2. 2
11. US DOT Description (Including Prop* Snipping Hunt. Hmrd Cltt*. tnd ID Numbtrl
(.r+f- ^ t'rttt)
Number r~,*7 i J\rf
CWM Profile Number
CWM Profile Number
CWM Profile Number
Ml tne contents ot mis consignmen*»,re fully end accurately described above By
. and labeled, and are in all respects in proper condition for transport by nignwav
nment regulations
16 GENERATOR'S C
proper snipping name-
according to appl
a program m place to reduce tne volume and toxieity of waste generated to tne degree I nave determined to oe
practicable metnod of treatment storage, or disposal currently available to me which minimxes tne present and
if I am a large quantity gt
economically practtcaMaMBplemtK
hMHMIIeYtl*
IKON, if I am a small quantity generator. I nave made a good laitn effort to mmimue my waste generation and select
to met and tnai I can afford
future threat tomjnurt
17 Treneporter 1 •cknooxeagemem of Heeeejt of MeMnete
Printed/Typed Meme
Montr) Oay
I/ I / I / I I
18.Tranapon*r 2 Aeknewtedoernent of Receipt of
Month Oey Xe
I I I I I I
1 S.Oiecrepency IndicMion Spec*
20.Fectlnv Owner or
mateneta covered by
Printed/Typed Neme
-------
H-21
HAZARDOUS WASTE MANIFEST
Moasa print or typo.
(A* Required By The Alabama Department of Environmental Management)
*W e*»r7*-**ett typewriter JForm «****. OMB No 20NKXM
Ewe* 9-3041
UNIFORM HAZARDOUS
ANWE9T
i* not required by Federal
WASTE MAN
4 Generator's Phone (
l'"l/ I" l-fl-4
Transporter 2 Company Name
W. oeeignated Facility Name and Srte AdJrea*
CHEMICAL WASTE MANAGEMENT, INC.
Emelle Facility
Alabama Highway 17 at Mile Marker 163
Emelle, Alabama 35459
0, 0|0|6|2| 2|4|6
11. US DOT Ottenmton HnetuOing fropff Stopping Mtmt. Hufrd CIMM. tnd ID Numttrl
CWM Profile Numbe
CWM Profile Number
CWM Profile Number
CWM Profile Number
16 GENERATOR'*
oroper shipping name
according to applicable)
if I am a large quantity
economically preet
'utur* threat to human
ttv
ii the contents of this consignment are tully and accurately described above by
and labeled, and are in all respects >n proper condition tor transport Dv highway
nment regulations
• program m place to reduce the volume and tomcity ot waste generated to tne oegree I nav* determined to Be
'•cncable method ol ireatmeni. storage, or disposal currently available to me which minimizes th* present and
M. it I am a small quantity generator. I have made a good lanh ellort 10 minimize my wast* generation and select
10 me and that I can atlord
latlord
Signature '
Month Orr
f i i, t/ r
V*
T
PJ
A
N
•
P
O
P.
T
P.
17 Tranaporter 1 Acknowtedgemejnt of
PrimooVTypod Name
\ t .,'•
Month Oay X*
rui'i 'i
18Tranaport*» 2 Aeknowtedgomom of ftecaMp* of Mewriala
Pnm«d/Tya*d Nemo
Signature)
Month 0»r Yt
I I I I I
19 Discrepancy Indication Space
20 Facility Owner or Operator Certification of receajl of hazardoua matenata
19
Printed/Typed Name
Signature
Month Otr
I'll
-------
H-22
Mease prim or type). Ifomi
HAZARDOUS WASTE MANIFEST
.*. (Aft Required By The Alabama Department of Environrtwotal Management)
moonomfft2-o»fhinp»writort Form Apenwd. OMB No Mto-oom Eipma 9-»«e
UNIFORM HAatMHUUUS
WASTE MANIFEST
uenemort rurn* ana nanny AODraee
- ™; - .;:/%; . , f
I the contents ot this consignment are fully and accurately described above by
. and labeled, and are in all respects m proper condition tor transport by highway
irnment regulations
> program m place to reduce the volume and tojiicity ot waste generated to the degree I nave determined to be
•Practicable method ol treatment, storage, or disposal currently available to me which mimmues the present and
I. if I am a small quantity generator. I have made a good laitn effort to minimize my waste generation and select
I that I can afford .
>'£*'
Signature
Month Off Yt,
i^i/i/irri
17Tn
PnrrWd/Tvped Nam*
Signature
Month On
I I I I I
2 Acfcnowtedgamt
Month Off Yt
19.0iaerepancy Indtcation Space
ZO.Fecilrry Owner or Operator Cernfleavon at
ot naxardoue matanale oevored by ttxe ineriifeai
•a noted m ftenv tB
Pnnted/Typed Name
Signature
Month Oay
I I I I t
-------
H-Z3
l-leaeo pnm or type.
HAZARDOUS WASTE MANIFEST
(Aft Required By The Alabama DepaiUnent of Environmental Management)
Form Approved. OMB No. lOK-Vm E«rca ».3>-«
UNIFORM HAZARDOUS
WASTE MANIFEST
it net required by Federal
j I i+ ; I — *-•-
4. Generator's Phone ( )
rranaporter i company Name
US EPA 10 Number
a. oeaionateg facility Name and Site
CHEMICAL WASTE MANAGEMENT. INC.
Emelle Facility
Alabama Highway 17 at Mile Marker 163
Email*, Alabama 35458
11. US DOT Description (Inctudtng Prop* Stopping Numt. Hutrd Clft*. »nd ID Number)
CWM Profile Number
CWM Profile Number
CWM Profile Number
mat the corttems 01 tnis ^nsignment are tully and accurately described above by
I. and labeled, and are in all respects m proper condition for transport by highway
nment regulations
if i am a lar
economically
future threattehuman
a program in place to reduce the volume and toxicny of waste generated to the degree I have determined to Oe
practicable method of treatment, storage, or disposal currently available to me which mimmmj the present and
. if I am a small quantity generator. I have made a good tanh effort to minimise my waste generation and select
to me and that I can afford _ -
0
N
T
I
U.Treneporter 2 AcHnoortedgemaot at Keeaipt of Matenato
Signature
Month Dor Ytt
I I I I I I
1 d.Diacrepeney Indteation Seaea
A
C
I
L
20 Facility Owner or Oparaioi Certifteatwn of receipt tt rtanrdoua matenala covered by true mervrreet
aa noted in item 19
PnmeayTypea Name
Signature
Month
I ' I
-------
H-24
HAZARDOUS WASTE MANIFEST
(AiJ»MuMi1 By The Alabama Department of Environmental Management)
$K>'. ^JP
r^A T*
US EPA 10 Number
" .'." 1/12 l£lC\1\ J\'
10. US EPA
Emelle Facility
Alabama Hiohway 17 at Mile Marker 163
Emetle, Alabama 35459
| A, L, D, 0, 0|0|6|2| 2|4|6|4
11. (JS OOT Ouucrivaon (I
Sfitpptng Mfmt. Htitrtt Clftt. ind IO Muir^tr>
CWM Prof,,. Numbar
16 GENEHATOffft
pr
according to
conteme-ot this consignment ara
and labeled, and are m all respects m
t regulations
accurately described above by
condition lor transport by highway
program in place 10 reduce the volume amftmcitv ol waste generated to the degree I have determined to Be
licable method or treatment, slorege. or disposal currently available to me which mimmites the present jnd
il I am a small quantity generator. Lheve made a good lailh ellorlto minimise my waste generation and select
1 »f»neomiB»smam of
2 Acunowtedgejmem of
A
C
1
l
T
20 Facility Owner or Operwor Certtficatien of ra««( of haaardoua mmna* eetanel fey 9m mamfeat •eae«« aa now) m Itajm 1».
Printed/Typed Name
Signature Month Oay /ea
| | | i | i
-------
H-25
HAZARDOUS WASTE MANIFEST
Mees* print or two.
By The Alabama Department of Environmental Management)
CMBND. :
ia not required by Federal
4. Generator's Phone (
'2 rV A/ ///*AJ> J•' I*~/Jt/V
1
/
>/~nc»T\JiyieO^-i fi yi;?i-^i--
•• 10. US EPA ID Num
CHEMICAL WASTE MANAGEMENT, INC.
Emelle Facility
Alabama Highway 17 at Mile Marker 163
Emelle. Alabama 35469
• A, L, 0, 0.0,0,8,21 2 4,6
11. US DOT Oaemption HI
Shipping Hunt. Hmnl Oau. »nd M3 Humburl
tne content* ot tmi con*gnn»em are iGAV and accurately describe* above by
and labeled, and are in all respect* irt'proper condition for transport by nignway
iment regulations
16 GEMCNA
proper shippmaj
according to
program in place to reduce the volume and tojiicity or waste generated to tne degree I nave determined to Be
ecticaole metnod oi treatment, storage, or disposal currently available to me which minimizes tne present and
I. if I am a small quantity generator. I have mad* a good tanh etforuo minimize my waste generation and select
K I am a large.
economically
'uture threat B»
tne
Month Oay X<
Moncn Oay Y,
Mantn Oay Y
20 FaoJIty Owner or Oparator
Printed/Typed Mama
Month Otr
1 I I I I
-------
H-26"
HAZARDOUS WASTE MANIFEST
By The Alabama Department of Environmental Management)
I- «• No. aMMOe. E*n*
Heeee prim or type.
UNIFORM _=^
WASTE MANI»«,fr
jil not required by Federal
w'-rA
4. Generator's Phone) (
A>>JMv/-4. />
2 Company fteme
CHEMICAL WASTE MANAGEMENT. INC.
Emelle Facility
Alabama Highvvev 17 at Mile Marker 163
Emelle. Alabama 35459
11. US Ml Omaqtwllndvding Prop* Shipping N*m.HtttrdClM*.ind ID Nua+tr)
CWM ProfHe Number
CWM Profile Number
CWM Profile Number
CWM Profile Number
the contents 01 this conscjnment are fully end accurately deacnbed above by
and labeled, and are m all respects m proper condition for transport by highway
regulations.
proper sh
according to
I' I am a Urg«
aconomicallypt
future threat
am in place to reduce the volume and toxicilv of wait* generated to the degree I rtave determined to Cw
icaMe method ol treatment, storage, or disposal currently available to me which mimmiies tne present and
il I am a small quantity generator. I have made a good laith etforup minimiu my wane generation and select
A
Mantfi Oar V«
I I I PIL. I I
of Keoeim of
Month Oar
I I I I I
i».P»acrepanc> indication Spaa
by thai
CO* C-^
-------
H-27
OUS WASTE MANIFEST
I By The Alabama Department of Environmental Management)
He*** prim or type. ffom
UNIFORM
WASTE MANtftST
.{ , - x r^-^
•'•-.' :
4. Generator's Phone (
US EPA 10 Number
CHEMICAL WASTE MANAGEMENT, INC
Email* Facility
Alabama Hi^ivwy 17 at Mill Marker 163
Emelle. Alabama 35459
;. CWM Profile Number
CWM Profile Number
CWM Profile Number
CWM Profit* Number
16 GENEMAT
proper
according to
If I am a large
economica
future threaUB
nts of mis consignment an tuily and aceVatvly deecnbed above by
and labeled, and are in all respects in proper condition for transport by rughwav
regulations. *
program m place 10 reduce me volume and toxicitv of waste generated to the degr** I hav* d*t*rmm*d to b*
•cable method of treatment, storage, or disposal currently available to me which mimmnes th* present and
!. it I am a small quantity generator. I have made a good faith eHort to mmimiz* my wast* generation and select
that I can afford "~?
Sitjnaw*~775 _, ~..,- Month Dor Yo\
PrUedyTypeJ fSST
18.Trafwp0nar2^
_ a *r*
Aetoowledgamani of
Stjnanwa
Month Day KM
3Z
ssaTT^afBEs;
HiLL-J •- -
SayVleWliW
sz
Oey
lii^V*Vy
•^•^•^pVBBvMMBrtBBa.flB.M.^.^11111]
19.0i^r«p.v»cy tm^tten
T
A
C
I
I
MFeciltty Owner or Operasor
Printed/typed Name)
of hejardpua matartala covered by tt«a
bgnatur*
Montn Oey
'''I'
-------
l^C*2l/*1
H-28
a Ganerator-s Mama and Ming Addrass
15. Spacial Handling Inatnjctiona and Additional Infofmatlon
16.
triatm^
rahipping nama and am claaamad, packad, markad. and laoatad, and art in all raapaeta m propar condition for tranaport by
highway according to appUcatt* IntamaMonal and national govammant ragulatlona, and Illinois raguMtana.
i£!£S' •mJL2m-l Ouiflt't1' 8««»n«orj«ho haa baan axamptad by sUtutaorragjjWlonfiomthadutytonialujawaatarnMmizat^
3002(bt of RCRA. I alao cactJfy tnat I haw a program in ptea to raduca ma voluma and toitetty of waata ganaratad to tna dagraa I raw* datarrmnad to t
_... .. ... , ^ ^.^^ ^ tmttmw,t ,toftfl, w^dlspoaal currant* avaMatoto to ma whtah n**ntaaa tna praaant and hrtu
C
S*gnatp>..- -
/tf
MonM 0*y
PrtntadTTypad
K'
1
' Ti!'iy "^^ """y ****'>**11 »«^.u»n^*.ca»aitJiTm ^~~
« • s i
IIPA COOT • MJIT I
-------
U-C62M1 H-29
Form Appfoy»a. QMB No J050-OO39 EJI
EPA Form 870O-22 (3-34)
'or u»» on «•» (i2-a«ai| iyp»aiii»
UNIFORM HAZARDOUS
1. Generator's US EPA O Na
Mamabonm the shaded ar««s« no
ederal lew
WASTE MANIFEST
3. Generator's Nam and Miianu Address
4. Generator's Phone (
5. Transporter 1 Company Name
/. Transporter 2 Company Name
9. De«gnated Facility Name and Site Address 10.
US EPA D Number
11. US DOT Descnptidr) (itcrurtng Proper S/uppmy Nam*. H»z«rt C/«M, and «> Mumberj
•-. T .,,./-
2= Cubic Yanla
T
A
N
S
O
ft
r
A
c
i
T
; L- ^snr^A^vanBia
ft , i^^E^BBfeVBBilllBJIBJIB^IBJI
IS. Special Handling inatructlona and Additional Information
16. GENERATOR'S CERTIFICATION: 1 hereby declare that the contents of this consignment are fully •
proper shipping name and are classified, peeked, marked, and labeled, and are in all respects in
3002{b) of RCRA, I also certify that 1 have a program m piece to reduce the volume and tcciclty
economically practicable and 1 have selected Vie method of treatment, storage, or disposal currer
ttwvMt to hunteVi heMltti «jWt ttw •nviranMBnL
t
17. Transporter 1 ActowerfedgeeMnt of Reese* of Mseenala
Printed/Typed Ne*ie^_ ^ Signeture- '""•
i». Transporter 2 *ckno»«edgeuienl of Fejiiilptol Metsnels
PrtntedfTyped Name Stgnetura
19. Discrepancy Indication Space
20. Facility Owner or Operator Certification of receipt of hszardous materials covered by this menit
Printed/Typed Name (signature
•l^RK5J|jlr<
m^BBBK^fflBHL' .'- '
••••^BBK3K,3g*' 's^t
od accurately described above by
igulations.
ty to make a waste minimization certification under Sectic
tty available to me which minimizes the present and futui
, X1 Date
// ^dp "Ti^"
,—\ Date
.x / ,v'c Month Day Yt
Dale " '
Month Day Yt
eat except as noted in item 19 Date
Month Day Yt
HCUNOS.217 / 782-3437
•24 K UR EMERGENCY AND SPU. AS&5TANU NUEBB^
OUTSOC UJ4OI& 800 / 424-8802 or 202 ' 426-26
DISTRBUTIOM: PART - 1 GENERATOR PART - 2 CPA PART - 3 FACUTY
PART - 4 TRANSPORTER
* tunme ID <•«•. ouvaii »
Ol -Ot B I1M
PART * 5 CPA PART - 6 GENERATOR
IVA COTT •
t4V • 9
-------
220O CHURCHILL ROAD. SPRINGFIELD. ILLINOIS 62794-9276 (217) 782-6761
PO BOX 19275
H-S32-O610
LPC628/81 "~30
Form designed tor UM on ante nz-txieM typewriter)
PA form sToo-aa iitov. »-aa
Form Aoorg^d OMB Mo 2060-0038. Exam
UNIFORM HAZARDOUS
WASTE MANIFEST
1 Generator's US EPA ID
Information m the shaded areas a
required by Federal law. but a requ
bymiroeiaw
3. Generator's Name and Mailing Address
4 Generator's Phone (
US EFA ID Number
5. .Transporter 1 Company Name
7. Transporter 2 Company Name
US EPA ID Number
US EPA ID Number
9. Designated Facility Name and Site Address
and /D Nunber)
Quantity irVt/vo
J. Additional Descriptions for
Wastes Loted Above
2 = Cubic Yar
15. Special Handling Instructions and Additional Information
16.
GENERATOR'S CERTIFICATION: I hereby declare that the contents o< trw consignment are fuUy and accurately descnbed above by
proper shipping name and are classified, peeked, marked, and labeled, and are in all respects in proper condition tor transport by highway
according to applicable international and national government regulations.
if l am a large quantity generator. I certify that I hew • program m place to reduce the volume and toxoty of waste generated U the degree I have determined to
economically practicable and that I have latertsd the practicable method of treatment storage, or dsjpoaal currently avaeabte to me whch minimizes the present
future threat to human health and the environment ON, 1 1 am a smeN quantity genefMOFtJ neve made a good faith jMBft to minimize my waste generation ana sa
the best waste ma
Date
and that I can afford.
Transporter 1 Acknowtedqement of Receipt of Matenala
Printed/Typed Name
>/
18. Transporter 2 Acknowledgement of Receipt of MateneJa
Pnnted/Typed Name
19. Discrepancy Indication Space
20. Facility Owner or Operator Certification of receipt of hazardous materials covered tty thai marxfeet except a* noted in item 19.
Date
Pnnted/Typed Name
Signature
Month Day
IN ILLINOIS 217 / 782-3837
*2« HOUR EMERGENCY AND SPILL ASSISTANCE NUMBERS*
OUTSIDE ILLINOIS BOO / 424-8002 or 202 ' 426-
DISTRIBUTION PART - 1 GENERATOR PART - 2 IEPA
PART - 3 FACILITY
PART - 4 TRANSPORTER
PART - 5 IEPA
PART - 6 GENERATOR
«ev 7
or -.Owvnr ot not -o • CMd S2SOOO Mr dBV 31 «o«Mr<
OCNf MATOft COTV - MKT 1-OO MOT MMOVI MffT 1 f«KIM BTT UNT*. COMFUTVO.
ji «• i>§ «in«i M aamu B ra «e»ey N*n •
) 5 vMr* Th« tarm rt« c
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220O CHURCMU. ROMX SfT9tCfEU3, LLMOB 62706 (217) 7*2-6761
i lor »•• OB «» nas»*Mmi «i j t>ft Fotm «7OO-aa f3-d M
20. FaeUlly OMMT or Oparator CantBeatton of ncilpt ot
•00 / 48liOOa or 202 / 426
MAT - 6 OBdUTDR
MNT-3MCUTY P»«T-4
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UMCBS 62700 (217)782-6761
form «70O-22 (3-«4|
Ooaqnatad FaciHy Mama and SMa
15.!
highway aooonMnQ to
I am a MHtl quantity
aooam of RCRA. i ate
w luHy mo 4wcwwiawy
In 0VQW condttlon tar traraport by
or raoudtton Horn ttw duty to
«• vofcm and Mviei^rofwi
cufiwOy
itiiiUaUmi certification under Saction
I to the dagnM I nava datanmnad to ba
i to ma •Men mlnimizaa tna pnjaant and future
ourace HMO* aoo / 424-0002 or 202 / 426-26?
2 P* WWT - 3 MCaJTY
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t onrrt or typ*.
{FofW
PO. BOX 19275
I (or UM on •*• (I2-OOCM
/*»»-<*i/O Ut7) ('82-0761
LPC628/81
*n --- ' ~~ '" ~ -- IT
o a
mqund by FMera) aw. but is raq
Generator's Name and Mailing Address
W4STE oiet
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H-34
"CALQON^
CALGON CARBON CORPORATION
1-1387
CALCON CARBON CORPORATION 120 EAST OCOEN AVE. HINSOALE, ILLINOIS 60521-3579 (312) 325-9090
June 30, 1987
Mr. Brian Bell
Canonie Environmental Services Corporation
800 Canonie Drive
Porter, IN 46304
Dear Brian:
Per your request, Calgon Carbon accepted approximately 30,000
pounds of spent carbon for reactivation at our Columbus, Ohio, facility
around September, 1986. Calgon Carbon also accepted approximately
15,000 pounds of spent carbon at our Neville Island facility around
the beginning of May, 1987. Both of these shipments were from the
Grey, Maine, project.
Please let me know if I can be of additional assistance.
Very truly yours,
Edward T. Ricketts
Technical Sales Representative
ETR:tl
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