xvEPA
                        United States
                        Environmental Protection
                        Agency
                     Andrew W Breidenbach
                     Environmental Research Center
                     Cincinnati OH 45268
                        Research and Development
                                 EPA-600/D-81-113  April 1981
ENVIRONMENTAL
RESEARCH   BRIEF
               Electron  Microscopy in Environmental Research
            Richard L. Boone1, Patrick J Clark1'2, James R Millette1, and Robert S. Safferman3
Background


Research conducted at the U.S. Environmental Pro-
tection Agency's Cincinnati laboratories is aided by a
shared electron microscope (EM) facility. This facility
includes two transmission electron  microscopes
(TEM), a scanning electron microsope (SEM), a con-
necting darkroom, and  a  specimen  preparation
laboratory containing light microscopes, vacuum
evaporators, and two ultramicrotomes.

Since inception, the new facility has been regulated
by a committee of principal scientists representing
the major program users. This shared operation, now
in its eighth year, has been a complete success. In
addition to enacting operating policies insuring equi-
table use of the facility, the committee's responsibil-
ities also include periodic  evaluation of the facility's
performance; EM operator certification; acquisition of
new or  additional  accessory equipment; and super-
vision of facility maintenance. The uniqueness is also
reflected in the fact that each program desiring use is
'R L Boone, P J Clark, and J R Millette are with the Health Effects
 Research Laboratory, Cincinnati, OH 45268
2P J Clark was formerly with the Municipal Environmental Research
 Laboratory, Cincinnati, OH 45268
3R S Safferman is with the Environmental Monitoring and Support Labora-
 tory, Cincinnati, OH 45268
                   responsible for providing  its own  personnel with
                   expertise in their specific area of interest.

                   The multi-faceted  needs were first met with the
                   acquisition of a JEOL* 100B TEM, which was later
                   upgraded  by the  addition  of  a  high-resolution
                   scanning attachment. This made specimen examina-
                   tion possible in scanning, scanning transmission, and
                   conventional  transmission  modes.  To add  micro-
                   analytical capability to the 100B, an energy dispersive
                   x-ray spectrometer  (EDS)  was  obtained, allowing
                   elemental analysis directly from observed specimens.
                   The recent development of even more sophisticated
                   microanalytical instrumentation resulted in replacing
                   the obsolete console of the ORTEC Delphi with that of
                   the ORTEC EEDS II multichannel analyzer and data
                   processor.

                   The increasing work load at the EM facility led to the
                   acquisition of a second transmission electron micro-
                   scope (the JEOL 10OCX) in 1 977 (Figure 1). Like the
                   100B TEM, the 100CX is equipped with a side-entry
                   goniometer and an ORTEC EDS detector The EEDS II
                   'The use of a specific manufactuer's name is for identification purposes only
                    and does not constitute endorsement by the U S Environmental Protection
                    Agency

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                                                                      Figure 1.
JEOL 100CX transmission
electron microscope and
the ORTEC EED8 II. The
EM to housed in a room
free from  EM-interfering
mechanical vibrations and
magnetic fields.
ETEC scanning electron micro-
scope with electron column
specimen  chamber  (right),.
instrument console and cath-
ode ray tube viewing screens
                                                        Figure 3.  LKB uttramicrotome.

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display console, obtained originally for the 10OB, can
be detached and moved to the 10OCX with minor ad-
justments.

The facility has also added an ETEC SEM to its group
of analytical tools (Figure 2).  The SEM  provides a
three-dimensional view and an added depth of field,
as  well  as  allowing  the  use  of  relatively large
samples. The SEM has recently been fitted with two
viewing screens allowing simultaneous specimen-
observation at both low and high magnification and
an EDS detector for use with the EEDS II console. The
EEDS II console is now equipped to obtain data on two
independent channels from separate electron micro-
scopes. This results in faster and more efficient use of
the microscopes without loss of  precise analysis.

Instruments are available for conventional- and cryo-
ultramicrotomy. Cryo-ultramicrotomy is used when
frozen thin sectioning of tissue is needed for the
microanalysis of certain elements which would be
leached by usual sectioning  techniques. For this
purpose the  LKB  Ultrotome IV (Figure 3) has been
fitted with an LKB CryoKit. An LKB* Ultrotome V is
available for preparing conventional sections.
Research Applications

Researchers are continually increasing their use of
the EM facility for studies in the areas of methods
development, air and water toxicology, and water
supply. The TEM, SEM, and EDS systems have been
very useful in the developmental work on asbestos
standards, and also the analyses of surface waters,
drinking  water, minerals, volcanic ash, and micro-
particulates from various sources.  High resolution
microscopy has had a large impact on the detection of
noncultivable viral agents associated with outbreaks
of gastroenteritis. It is also important in inhalation
toxicology studies  to  detect  changes  in tissue
morphology after animal exposure to smoke and dust
particulates. Moreover, research concerning ultra-
structural tissue changes related to the ingestion of
trace metals has been  heavily dependent  on EM
analysis.


Asbestos

Inhalation of asbestos fibers is a known cause of lung
cancer. Ingestion of asbestos is suspect as a cause of
gastrointestinal cancer among workers occupation-
ally  exposed to asbestos,  and possibly  may  be a
hazard to those who have ingested asbestos in drink-
ing water. The TEM-EDS  system  is  used as  a
complete analytical tool in the identification, charac-
terization, and determination of the concentration of
asbestos fibers in drinking water supplies throughout
the United States, TEM is required because asbestos
fibers which are as small as 300A, cannot be resolved
using the conventional light microscope. The exact
mineral variety, elemental composition, and crystal
structure  are  determined  using TEM  by  direct
morphology, selected area electron diffraction, and
EDS (Figures 4, 5, and 6).
Figure 4.  Electron micrograph of chrycotile asbestos fiber* in
         prepared standard showing distinct morphology and
         •elected area electron diffraction pattern (upper left).
Figure 5.  Electron micrograph of amptiibole asbestos fiber in
         water from distribution system with selected area
         electron diffraction pattern (upper right).

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Figure 6.  Characteristic- spectra of chrysotile asbestos dis-
         played on the ORTEC EEDS II console.

The SEM has been extremely useful in the examina-
tion  for  surface  deterioration  of asbestos-cement
(A/C) products (water distribution pipes and roofing
tiles).  Continued surface  deterioration  commonly
results in the release of asbestos fibers into drinking
water supplies. Health and economic factors result-
ing from the  deterioration of A/C materials have
stimulated  research on corrosion-preventive  com-
pounds, such as zinc orthophosphate. The SEM-EDS
can be used to determine the coating effectiveness of
these corrosion inhibitors (Figure 7a,  b, and c).

Size characterization of asbestos fibers according to
length and., width involves EM analysis. It is believed
that  the size of the fiber, especially the length, may
have an effect on its ability to cause cancer. It is there-
fore important to characterize the asbestos fibers
in prepared standards used for cancer research. Once
it is confirmed that a standard contains fibers of a
certain  size range, the effects of fiber  size in the
biological testing can be better ascertained. Similar
characterization has also been applied to fibrous or
fibrous-like clay particulates.

Monitoring drinking water for asbestos utilizes TEM
analysis. Therefore, quality assurance pertaining to
sample   preparation  and  analytical  technique is
needed.  To fulfill such  a need, asbestos standards
similar to known indigenous fiber conc'entrations and
size distributions are being prepared to be sent to
laboratories analyzing water samples for asbestos.


Cardiovascular Tissue Changes
EM studies  are used in the  evaluation of environ-
mental factors related to ultrastructural cardiovas-
cular tissue changes. The ultra-microtome, modified
with a CryoKit, can obtain  ultra-thin frozen tissue
sections of the ventricular wall of the heart, which are
then analyzed by TEM-EDS. Observations are made
for  any soluble toxic chemicals that may have accu-
mulated  in the tissue, with special attention given to
binding in the mitochondria. Morphometric analyses
of  electron  micrographs are also being used to
observe changes in the nuclear pole areas for early
detection of cardiovascular disease (Figure 8).


Virus Detection
Electron  microscopy  plays a  crucial role  in  the
detection of noncultivable  viral  agents,  many of
Figure 7.  (a) SEM photograph of surface of unused A/C distribution pipe, (b) SEM photograph of surface of corroded A/C pipe,
         (c) SEM photograph of surface of A/C pipe coated with zinc orthophosphate.

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Figure 8.  Electron micrograph of nuclear pole region found in
         rat ventricular wall. (N) nucleus; (M) mitochondria;
         (G)  Golgi  apparatus; (NM) nuclear membrane (A.
         Tonti).
which have been implicated in outbreaks of gastro-
enteritis. EM studies at this facility have detected a
number  of  these virus particles in fecal  material
obtained from afflicted humans or animals (Figures 9
and  10).


Algal Identification
Much of the structural detail of microalgae is so small
it can be resolved only by TEM or SEM analyses. Both
procedures  have been  used to examine  algae from
surface waters and to prepare identification manuals
for field biologists to determine the effects of pollu-
tants on the species composition of algal communi-
ties  in receiving waters (Figures 11  and 12).


Intra-Cellular Deposition of Particulates

When animals are exposed to diesel exhaust fumes,
the emitted  product in whole paniculate form affects
certain target  organs  of the body. The lung  is  a
primary receptor for absorption  of this paniculate,
which is  phagocytized by  selective cells.  Electron
microscopy  magnifies the ingested paniculate and
the  surrounding area of deposition (Figure 13). In
contrast to that seen with the light microscope, this
                                                      enables the laboratory to obtain a more detailed per-
                                                      spective of intra-cellular relationships.


                                                      Summary

                                                      There  is no  doubt that the TEM,  SEM,  and  EDS
                                                      systems are powerful analytical tools for structural
                                                      determination  and chemical  identification.  These
                                                      systems support important objectives of the research
                                                      groups  at  ERC-Cincinnati   through their various
                                                      engineering, biological and mineralogical applica-
                                                      tions.
Figure 9.  Rotavirus: "complete" or "smooth" double-shelled
         virions can be seen in the upper portion of the elec-
         tron micrograph, while a group of "rough" single-
         shelled virions appear below. Two stain-penetrated
         virions of each type can be seen (F. Williams).
Figure 10.  Electron micrograph of astrovirus particles, some
          possessing a distinctive star-shaped surface mor-
          phology and smaller parvovirus particles showing
          no such distinctive morphology (F. Williams).

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Figure 11,   Scanning  electron micrograph of the  diatom,
            Stephanoditcut hantztchll, showing the micro-
            structure of the cell wall (B. McFarland).
                                                             Figure 12.  TransmiMion electron micrograph of the *mall dia-
                                                                        tom, Thalattlotlrapteudonana, common in eutro-
                                                                        phic water* (C, Weber).
                                                             Figure 13.  Tran*mi**ion electron micrograph of rat lung ti»-
                                                                        *ue. Arrow point* to a macrophage that ha* phago-
                                                                        cytized depo*ited die*el fuel exhaurt particulate*
                                                                        inhaled into the lung* (H. Ball).
                                                                                      .-. u* eovewMBff nwnma orrtct HM -7»7-«l2/7
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