-------
Triangle Laboratories, inc.
Run Log
CO
Instrument ID Column TYPO Column ID Plot Name
Inj. Vol. Acquisition
Signature
G/C
?S"/1?
Date
Filename
Date*
Time*
Project #
Sample*
No.
Client Sample ID
Syr
332
Operator/Date
Comments'
2L
to^h
, o
u
* Transcribed from chromatographic data
** Dated initials required
srvr1/qa/forms/hrrunlog.doc (02/05/97)
ConCalDue:
ConCalDue:
98
Pann-
-------
Triangle Laboratories, Inc.
Run Log
_.
Instrument ID Column Type Column ID Plot Name
Inl. Vol. Acquisition 6/C
d-O^) )C£e»«>£/"jT~"~ Kf Co*Jf--'n~ -\
tL/frt ' $s^s£-e^ 1-0-^ 7
Signature Date
Transcribed from chromatographic data
** Dated initials required
5rvr1/qa/forms/hrrunlog.doc (02/05/97)
ConCal Due:
ConCal Due:
Paae:
, 99
-------
Triangle Laboratories, Inc.
Run Log
en
Instrument ID
Column Type
on
Column ID
Plot Name
Ttf
Acquisition
Signature
G/C
Date
Filename
Date*
Time*
Project #
Sample*
No.
Client Sample ID
Syr
332
O[)era(or/D«te
Comments"
6. L
1-1-
Ms
M
V-
Ut
Transcribed from chromatographic data
** Dated initials required
srvr1/qa/forms/hminlog.doc (02/05/97)
ConCal Due:
ConCal Due:
Page:
80
-------
SAMPLE
DATA
Triangle Laboratories, Inc. '
801 Capttola Drive P.O. Box 13485
Durham, NC 277134411 Research Triangle Park, NC 27709-3485
919444-5729 Fax i 9194444491
34
-------
TRIANGLE LABORATORIES, INC.
Sample Result Summary for Project 43057
Method 23X Full Screen Analyses (DB-5)
Data File
Sample ID
Units
Extraction Date
Analysis Date
Instrument
Matrix
Extraction Type
Analytes
2378-TCDD
12378 -PeCDD
123478-HxCDD
123678-HXCDD
123789-HxCDD
1234678-HpCDD
OCDD
2378-TCDF
12378 -PeCDF
23478-PeCDF
123478-HXCDF
123678-HXCDF
234678-HXCDF
123789-HxCDF
123467 8-HpCDF
1234789-HpCDF
OCDF
TOTAL TCDD
TOTAL PeCDD
TOTAL HxCDD
TOTAL HpCDD
TOTAL TCDF
TOTAL PeCDF
TOTAL HxCDF
TOTAL HpCDF
Other Standards
37C1-TCDD
13C12- PeCDF 234
13C12-HXCDF 478
13C12-HXCDD 478
13C12- HpCDF 789
S975807
TLI M23 Blank
ng
09/06/97
09/10/97
S
XAD
Soxhlet
(0.003)
(0.004)
(0.006)
(0.005)
(0.005)
0.03
{0.02}
0.007
(0.003)
0.007
0.03
{0.008}
0.01
(0.004)
0.04
{0.01}
{0.02}
0.008
{0.01}
0.04
0.03
0.01
0.007
0.05
0.06
Percent Recovery
98.6
93.3
90.4
82.3
75.1
S975808
I-M23-1
ng
09/06/97
09/10/97
S
M2 3 TRAIN
Soxhlet
{0.004}
0.01
0.02
0.04
0.05 PR
0.72
44.5
0.04 B
0.008
0.02 B
0.06 PRB
0.02 B
{0.02} PRB
0.007
0 . 12 PRB
0.04 B
0.16 B
0.05
0.07
0.45
1.6
0.14
0.12
0.19
0.30
Summary (% Rec)
97.6
93.2
94.6
88.0
83.6
Other Standards Percent Recovery Summary (% Rec)
13C12-HxCDF 789 80.9 91.3
13C12-HxCDF 234 95.7 99.0
Internal Standards Percent Recovery Summary (% Rec)
13C12-2378-TCDF 90.5 98.5
13C12-2378-TCDD 76.0 89.0
13C12-PeCDF 123 87.2 95.5
13C12-PeCDD 123 93.1 103
S975809
0-M23-1
ng
09/06/97
09/10/97
S
M23TRAIN
Soxhlet
(0.003)
(0.005)
(0.006)
0.01
0.02
0.06 B
0.53
0.02 B
{0.006}
{0.01} B
0.04 PRB
0.01 B
0.02 PRB
(0.004)
{0.07} PRB
0.04 B
0.04 B
0.007
{0.04}
0.12
0.10
0.03
0.05
0.12
0.04
96.1
86.1
87.3
81.0
88.7
58.1
61.4
69.4
63.2
67.1
68.2
Page 1
09/12/97
S975810
0-M23-2
ng
09/06/97
09/10/97
S
M23TRAIN
Soxhlet
(0.006)
(0.008)
(0.01)
{0.02}
(0.01)
{0.04} B
0.19 B
0.03 B
(0.006)
(0.006)
0.04 B
0.01 B
0.02 PRB
(0.008)
PRB
0.07
0.02
0.06
0.02
0.03
0.08
0.04
0.04
(0.006)
0.11
0.12
98.8
85.1
92.1
91.9
84.9
54.3
62.0
62.4
55.6
57.6
60.5
Triangle Laboratories, Inc.® Analytical Services Division
801 Capitola Drive • Durham, North Carolina 27713
Phone: (919) 544-5729 • Fax: (919) 544-5491
Printed: 0851 09/12/97
-• w % O O
-------
Data File
Sample ID
Units
Extraction Date
Analysis Date
Instrument
Matrix
Extraction Type
TRIANGLE LABORATORIES, INC.
Sample Result Summary for Project 43057
Method 23X Full Screen Analyses (DB-5)
S97S807
TLI M23 Blank
ng
09/06/97
09/10/97
S
XAD
Soxhlet
S975808
I-M23-1
ng
09/06/97
09/10/97
S
M23TRAIN
Soxhlet
S975809
0-M23-1
ng
09/06/97
09/10/97
S
M23TRAIN
Soxhlet
Internal Standards Percent Recovery Summary (% Rec)
13C12-HXCDF 678 102
13C12-HXCDD 678 87.2
13C12-HpCDF 678 78.9
13C12-HpCDD 678 80.2
13C12-OCDD 55.7
102
93.6
71.1
78.3
60.5
68.8
65.4
42.3
50.4
36.0
Page 2
09/12/97
S975810
0-M23-2
ng
09/06/97
09/10/97
S
M23TRAIN
Soxhlet
65.7
58.8
41.3
44.9
27.5
Triangle Laboratories, Inc.® Analytical Services Division
801 Capitola Drive • Durham, North Carolina 27713
Phone: (919) 544-5729 • Fax: (919) 544-5491
Printed: 0821 09/12/97
--•- 36
-------
TRIANGLE LABORATORIES, INC.
Sample Result
Summary for Project
Method 23X Full Screen Analyses
Data File
Sample ID
Units
Extraction Date
Analysis Date
Instrument
Matrix
Extraction Type
Analytes
2378-TCDD
12378-PeCDD
123478-HxCDD
123678-HxCDD
123789-HxCDD
1234678-HpCDD
OCDD
2378-TCDF
12378-PeCDF
23478-PeCDF
123478-HxCDF
123678-HxCDF
234678-HxCDF
123789-HxCDF
1234678-HpCDF
1234789-HpCDF
OCDF
TOTAL TCDD
TOTAL PeCDD
TOTAL HXCDD
TOTAL HpCDD
TOTAL TCDF
TOTAL PeCDF
TOTAL HxCDF
TOTAL HpCDF
Other Standards
37C1-TCDD
13C12- PeCDF 234
13C12-HXCDF 478
13C12- HXCDD 478
13C12- HpCDF 789
Other Standards
13C12 -HxCDF 789
13C12 -HxCDF 234
S975811
0-M23-3
ng
09/06/97
09/10/97
S
M2 3 TRAIN
Soxhlet
{0.003}
0.005
0.008
0.02
{0.01} PR
0.06 B
0.13 B
0.02 B
0.007
0.01 B
0.06 PRB
0.02 B
0.02 PRB
(0.003)
0.09 PRB
{0.03} B
0.06 B
0.01
0.03
0.15
0.06
0.03
0.06
0.17
0.09
Percent Recovery
98.4
88.6
98.2
87.9
91.3
Percent Recovery
120
173
S975816
0-M23-FB
ng
09/06/97
09/11/97
S
M23TRAIN
Soxhlet
(0.01)
(0.01)
(0.01)
{0.02}
{0.02} PR
0.06 B
0.11 B
(0.006)
{0.01}
0.03 B
0.07 B
0.03 B
0.03 PRB
(0.01)
{0.09} PRB
0.04 B
0.07 B
{0.02}
0.02
0.06
0.06
(0.006)
0.03
0.13
0.10
Summary (% Rec)
123
112
91.1
82.4
85.4
Summary (% Rec)
32.2 V
34.1 V
Page 3
43057 09/12/97
(DB-5)
S975817
0-M23-RB
ng
09/06/97
09/11/97
S
M23TRAIN
Soxhlet
(0.004)
0.01
(0.006)
0.02
{0.02} PR
0.08 B
0.11 B
{0.006}B
{0.008}
0.02 B
0.06 PRB
0.02 B
0.03 PRB
0.007
0.11 B
0.04 B
0.06 B
{0.01}
0.05
0.15
0.13
{0.006}
0.02
0.18
0.17
107
102
90.2
91.6
89.0
66.8
76.9
Internal Standards Percent Recovery Summary (% Rec)
13C12-2378-TCDF
13C12-2378-TCDD
13C12- PeCDF 123
13C12- PeCDD 123
184
163
161
170
49.5
34.3 V
44.9
54.8
88.5
76.4
89.1
99.3
Triangle Laboratories, Inc.® Analytical Services Division
801 Capitola Drive • Durham, North Carolina 27713
Phone: (919) 544-5729 • Fax: (919) 544-5491
Printed: 0821 09/12/97
-•-- 37
-------
TRIANGLE LABORATORIES, INC.
Sample Result Stannary for Project 43057
Method 23X Full Screen Analyses (DB-5)
Page 4
09/12/97
Data File
Sample ID
Units
Extraction Date
Analysis Date
Instrument
Matrix
Extraction Type
Internal Standards
13C12-HXCDF 678
13C12-HXCDD 678
13012-HpCDF 678
13C12-HpCDD 678
13C12-OCDD
S975811
0-M23-3
ng
09/06/97
09/10/97
S
M23TRAIN
Soxhlet
Percent Recovery
187
173
105
109
65.1
S975816
0-M23-FB
ng
09/06/97
09/11/97
S
M23TRAIN
Soxhlet
Summary (%
34.7 V
40.1
32.7
38.2
36.9
S975817
O-M23-RB
ng
09/06/97
09/11/97
S
M23TRAIN
Soxhlet
Rec)
74.0
78.2
56.7
61.3
60.9
{Estimated Maximum Possible Concentration}, (Detection Limit)
Triangle Laboratories, Inc.® Analytical Services Division
801 Capitals Drive • Durham, North Carolina 27713
Phone: (919) 544-5729 • Fax: (919) 544-5491
Printed: 08:21 09/12/97
-------
TRIANGLE LABORATORIES, INC.
Sample Result Summary for Project 43057
Method 23X (DB-225)
Data Pile
Sample ID
X973081
TLI M23 Blank
X973082 X973083
I-M23-1 O-M23-1
ng ng
09/06/97 09/06/97
09/11/97 09/11/97
X X
M23TRAIN M23TRAIN
Soxhlet Soxhlet
{0.02} B {0.008)3
Internal Standards Percent Recovery Summary (% Rec)
13C12-2378-TCDF 72.6 73.7 59.8
Units
Extraction Date
Analysis Date
Instrument
Matrix
Extraction Type
Analytes
2378-TCDP
ng
09/06/97
09/11/97
X
XAD
Soxhlet
0.005
Page 1
09/12/97
P973845
0-M23-2
ng
09/06/97
09/12/97
P
M23TRAIN
Soxhlet
(0.02)
52.4
Triangle Laboratories, Inc.® Analytical Services Division
801 Capitola Drive • Durham, North Carolina 27713
Phone; (919) 544-5729 - Fax: (919) 544-5491
Printed: 15:09 09/12/97
-------
Data Pile
Sample ID
Units
Extraction Date
Analysis Date
Instrument
Matrix
Extraction Type
Analytes
2378-TCDF
TRIANGLE LABORATORIES, INC.
Sample Result summary for Project 43057
Method 23X (DB-225)
Page 2
09/12/97
P973846
0-M23-3
ng
09/06/97
09/12/97
P
M23TRAIN
Soxhlet
0.02 B
P973847
0-M23-RB
ng
09/06/97
09/12/97
P
M23TRAIN
Soxhlet
(0.01)
Internal Standards Percent Recovery Summary (% Rec)
13C12-2378-TCDF 148 67.7
{Estimated Maximum Possible Concentration}, (Detection Limit)
Triangle Laboratories, Inc.® Analytical Services Division
801 Capitda Drive • Durham, North Carolina 27713
Phone: (919) 544-5729 • Fax: (919) 544-5491
Printed: 15:09 09/12/97
-~ 40
-------
TLI Project: 43057
Client Sample: TLI M23 Blank
Method 23 PCDD/PCDF Analysis (a)
Analysis File: S975807
Client Project
Sample Matrix:
TLI ID:
Sample Size:
Dry Weight
GC Column:
As-PHfiLT-puiMr
XAD
TLI Blank
1.000
n/a
DB-5
•Vf"
Date Received:
Date Extracted:
Date Analyzed:
Dilution Factor
Blank File:
Analyst
II
09/06/97
09/10/97
n/a
S975807
ML
Spike File:
ICak
ConCal:
% Moisture:
% Lipid:
% Solids:
SPX23704
SF56117
S975797
n/a
n/a
n/a
. Aftaiytes, -^^ , -^ v % ^
2,3,7,8-TCDD
!A3,7,8-PeCDD
1,23,4,7,8-HxCDD
1,^3,6,7,8-HxCDD
1,^3,7,8,9-HxCDD
1,23,4,6.7,8-HpCDD
1,^3,4,6,7,8,9-OCDD
W.7.8-TCDF
1,23,7,8-PeCDF
2,3,4,7,8-PeCDF
1,23,4,7,8-HxCDF
1,2^,6,7,8-HxCDF
2^.4,6,7,8-HxCDF
1,2^,7,8,9-HxCDF
1,2^,4,6,7,8-E^CDF
1,2^,4,7,8,9-HpCDF
1,2^,4,6,7.8,9-OCDF
&^;^£*?~^?
Total TCDD
Total PeCDD
Total HxCDD
Total HpCDD
Total TCDF
Total PeCDF
Total HxCDF
Total HpCDF
"^'''X'1^ ^*|n** ^Sl^^^^:wt,^^;^lSW^^^^|!| |^s'^d»^^
ND 0.003
ND 0.004
ND 0.006
ND 0.005
ND 0.005
0.03 1.14
EMPC 0.02
0.007 0.68
ND 0.003
0.007 1.76
0.03 1.09
EMPC 0.008
0.01 1.13
ND 0.004
0.04 0.96
EMPC 0.01
EMPC 0.02
;~ - JyAmt, #8j^«to»&<*v ^^r^MPtef?^^^?^^
0.008 1
EMPC 0.01
0.04 1 0.06
0.03 1 0.05
0.01 2
0.007 1
0.05 3 0.08
0.06 3 0.07
32:02
20:25
25:30
28:22
29:00
31:11
—
Page 1 of2
Triangle Laboratories, Inc.®
801 Capitola Drive • Durham, North Carolina 27713
Phone: (919? 544-5729 • Fax: (919) 544-5491
Printed: 1455 09/11/97
-------
TLI Project: 43057
Client Sample: TLI M23 Blank
Method 23 PCDD/PCDF Analysis (a)
Analysis File: S975807
'^" *!> '^sjSfl^wS'wF's^T^ ^wisti
13C,,-2,3,7,8-TCDF
13Cu-2^,7,8-TCDD
13Cu-U,3,7,8-PeCDF
l3Cii-lA3,7,8-PeCDD
13Ca-l,2,3,6,7,8-HxCDF
uCu-lA3,6,7,8-HxCDD
uC1I-lA3,4,6,7,8-HpCDF
I3Cu-l,i3,4,6,7,8-HpCDD
13Cu-lA3,4,6,7,8,9-OCDD
^KVJ?%vTJ'v^'*<*>*s*^^> **S?§5^S^
3.6 90.5
3.0 76.0
3.5 87.2
3.7 93.1
4.1 102
3.5 87.2
3.2 78.9
3.2 80.2
4.5 55.7
^&*4
Triangle Laboratories, Inc.*
801 Capitals Drive • Durham, North Carolina 27713
Phone: (919) 544-5729 • Fax: (919) 544-5491
Printed: 14-55 09/11/97
J- 42
-------
Data Review By:
lull
Calculated Noise Area:
1.48
The Total Area for each peak with an ion abundance ratio outside
ratio limits has been recalculated according to method requirements.
Page No.
09/11/97
Listing of S975807B.dbf
Matched GC Peaks / Ratio / Ret. Time
Compound/
M_z QC.Log Omit Why ..RT. OK Ratio Total.Area... Area.Peak.1.. Area.Peak.2.. Rel.RT Compound.Name.. ID.
Flags.
TCDF
304-306
D
D
D
D
304-306
13C12-TCDF
316-318
316-318
TCDD
320-322
D
320-322
DC
DC
DC
DC
D
D
D
D
DC
DC
DC
DC
D
DC
DC
DC
DC
DC
DC
DC
DC
DC
DC
DC
DC
NL
SN
SN
SN
SN
SN
SN
SN
WH
2
NL
WL
4
NL
SN
SN
SN
SN
SN
SN
SN
SN
SN
SN
SN
WH
WH
1
0:
16:
17:
18:
18:
19:
19:
19:
20:
22:
22:
00
57
57
07
53
30
44
55
25
20
44
0.
RO
RO
RO
RO
RO
RO
RO
RO
65-0.89
0.
1.
1.
0.
1.
1.
0.
0.
0.
0.
0.
12
17
35
48
26
54
89
78
68
53
99
Peaks
0:
19:
19:
19:
20:
20:
00
11
33
54
24
54
0.
RO
RO
RO
0.
2.
1.
2.
4.
6.
4.
6.
13.
5.
2.
20.
16
16
31
92
16
27
72
92 3.03
19 5.36
61
69
11
65-0.89
5.
0.
0.
0.
0.
0.
Peaks
0:
18:
18:
19:
19:
20:
20:
21:
21:
21:
22:
00
16
44
15
55
21
36
01
16
39
03
22:07
22:
22:
22:
:19
:37
:44
0.
RO
57
72
90
73
74 5
60
5
65-0.89
1.14
0.89
RO
RO
RO
RO
RO
RO
RO
RO
RO
RO
RO
RO
1.
7.
11
10
2.05
4.52
1.
0.
,05
,47
0.41
0.58
1.95
1,
0
2
0
.35
.52
.20
.69
Peak
0.
37.
6.
26.
,711.
21.
12
82
32 3.23
14 11.03
00 2,422.50
68 9.43
0.823-1.104
0,
.000
0.831
0.880
0
0
0
.888
.926
.956
0.967
3.89 0.976
7.83 1.001 2378-TCDF AM
1
1
.095
.114
0.951-1.049
0
0
3.57 0
15 . 11 0
3,288.50 1
15.77 1
.000
.940
.958
.975
.000 13C12-2378-TCDF ISO
.025
,765.14
0.12
9.47 4.47
5.
15
0.18
2.64
1.
1.
0.
.61
,31
46
3.75
0.
,57
0.35
0.55
0.74
1,
.13
2.25
0.857
0
5.00 0
0
0
0
0
0
0
1
1
1
1
1
1
1
-1.061
.000
.861
.883
.907
.939
.959
.971
.991
.002 2378 -TCDD AN
.020
.039
.042
.052
.066
.071
9.47
Triangle Laboratories, Inc.® Analytical Services Division
801 Capitals Drive • Durham, North Carolina 27713
Phone: (919) 544-5729 • Fax: (919) 544-5491
Printed: 14:55 09/11/97
M f\
-------
Page No.
09/11/97
Listing of S975807B.dbf
Matched GC Peak* / Ratio / Ret.. Tine
Compound/
M_2.... QC.Log 0»it Why ..RT. OK Ratio Total.Area... Area.Peak.1.. Area.Peak.2.. Rel.RT Compound.Naac
ID.. Flags.
37C1-TCDD
326
328
13C12-TCDD
332-334
DC ML 0:00
19:40
21:14
2 Peaks
DC ML 0
:00
0.
RO
19:52
332-334
PeCDF
340-342
D
21
21
21
22
:00
:13
:35
:19
80
RO
3
3
0
17
,223
,240
.07
.32 17.32
.15 3,223.15
.47
65-0.89
25
0
0
0
0
3
5 Peaks
DC HI. 0
DC SN 22
DC SN 23
D SN 23
DC SN 23
DC SN 24
DC SN 24
DC SN 24
DC SN 24
DC SN 24
25
:00
:38
:25
:50
:58
:11
-.38
:43
-.53
-.56
:30
DC SM 25:40
340-342
13C12- PeCDF
352-354
352-354
PeCDD
356-358
O
DC SN 26
DC SN 26
:10
:28
1.
RO
RO
RO
RO
RO
RO
RO
RO
BO
RO
RO
RO
.25
.86
.80 4
.78 3
.92
.23
8
32-1.78
0
1
0
1
3
1
2
2
0
0
1
2
0
1
.89
.21
.07
.28
.19
.57
.33
.64
.72
.17
.76
.76
.87
.30
1 Peak
DC NL 0
23
24
24
24
25
25
26
:00
:49
:21
:42
:53
:01
:29
:28
1.
RO
RO
0
20
,787
,879
57
3
.14
.47 9.47
.66 2,133.57
.19 1,696.09
.53 29.78
.75 6.85
0.
0.
11.00
2,654.09
2,183.10
32.50
2.12
906-1.094
0.000
0.927
1.001 37C1-TCDD
SDR1
906-1.094
0
0
0
1
1
1
.000
.936
.990 13C12-1234-TCDD
.000 13C12-2378-TCDD
.017
.052
RSI
IS1
,748.60
TCDD / PeCDF Follows --
0
3
0
10
2
4
3
4
1
0
9
4
0
2
9
.13
.54
.10
.18
.14
.19
.72
.11
.09
.81
.48 6.04
.21
.95
.88
.48
32-1.78
1
1
1
1
1
1
1
1
7 Peaks
DC NL 0
23
D SN 24
DC SN 24
:00
:58
:44
:54
1.
RO
RO
RO
RO
.00
.46
.26
.44 4
.34
.60
.46 4
.34
9
32-1.78
1
1
2
3
.14
.13
.59
.32
0
62
22
,731
20
31
,282
10
.13
.35 36.99
.00 13.37
.50 2,794.06
.34 11.65
.38 19.30
.56 2,541.48
.58 6.06
0.
3.44
0.
25.36
10.60
1,937.4*
8.69
12.08
1,741.08
4.52
909-1.079
0
0
0
0
0
0
0
1
1
1
1
1
1
1
.000
.916
.948
.965
.970
.979
.997
.001 12378- PeCDF
.007
.009
.032 23478-PeCDF
.039
.059
.072
AN
AM
838-1.162
0
0
0
1
1
1
1
1
.000
.964
.986
.000 13C12- PeCDF 123
.007
.013
.032 13C12- PeCDF 234
.072
IS2
SOR2
,160.71
PeCDF / PeCDD Follows "
0
11
7
0
.13
.57 7.03
.14
.94
0.
6.24
921-1.026
0
0
0
0
.000
.927
.957
.963
Triangle Laboratories, Inc.® Analytical Services Division
801 Capitola Drive • Durham, North Carolina 27713
Phone: (919) 544-5729 • Fax: (919) 544-5491
Printed: 14:55 09/1 1/97
44
-------
Page No.
09/11/97
Listing of S975807B.dbf
Matched GC Peaks / Ratio / Ret. Tine
Compound/
M_Z QC.Log Oait Why ..RT. OK Ratio Total.Area... Area.Peak. 1.. Area.Peak.2.. Rel.RT Compound.Name.. ID.. Flag*.
D
356-358
13C12-PeCDD
368-370
368-370
HxCDF
374-376
D
M
M
D
D
374-376
13C12-HXCDF
384-386
384-386
0
DC
DC
DC
DC
DC
DC
DC
D
DC
DC
D
DC
DC
DC
D
DC
DC
DC
DC
DC
DC
SN
SN
SN
SN
HH
1
NL
2
NL
WL
SN
SN
SN
SN
SN
SN
SN
SN
SN
SN
HH
HH
HH
5
NL
8
25:04
25:23
25:33
25:52
26:36
Peak
0:00
25:51
25:59
Peaks
0:00
27:13
27:22
27:32
27:50
28:00
28:04
28:22
28:29
28:36
29:00
29:10
29:28
29:42
29:48
29:53
29:58
30:03
30:08
30:17
Peaks
0:00
27:22
27:30
28:22
28:28
28:46
28:59
29:41
29:56
Peaks
RO
RO
RO
RO
1.
RO
1.
RO
RO
RO
RO
RO
RO
RO
RO
RO
RO
RO
RO
RO
0.
RO
RO
RO
1.
1.
2.
1.
1.
99
98
13
48
85
6.
2.
3.
3.
1.
11.
30
42
24
30
50
57
32-1.78
1.
1.
1.
00
52
57
0.
2,831.
274.
3,106.
05-1.43
1.
1.
1.
1.
1.
0.
1.
1.
1.
1.
1.
0.
0.
1.
1.
0.
2.
1.
3.
0.
92
89
15
02
45
62
20
09
47
23
13
25
45
76
25
31
42
40
02
52
2.
1.
10.
20.
5.
2.
1.
28.
11.
4.
16.
0.
1.
2.
8.
0.
2.
2.
2.
0.
87.
12
82 1,707.75
19 167.61
01
37
77
70 5.72
47 11.33
08
64
10
80 15.00
42 7.51
29
45 8.74
51
10
60
16
38
15
21
49
90
84
43-0.59
0.
0.
0.
0.
0.
0.
0.
0.
0.
56
61
49
50
,51
62
,50
50
,32
4.
8.
20.
3,106.
3,584.
6.
3,127.
2,300.
5.
28
29 3.37
48 6.72
44 1,035.27
38 1,213.22
37 2.60
95 1,039.98
71 765.04
66 1.91
0.
1,124.07
106.58
0.
4.98
11.15
13.80
5.10
7.71
0.
5.49
13.76
2,071.17
2,371.16
4.22
2,087.97
1,535.67
6.06
0.970
0.982
0.988
1.001 12378-PeCDD
1.029
845-1.155
0.000
1.000 13C12-PeCDO 123
1.005
957-1.053
0.000
0.956
0.961
0.967
0.978
0.984
0.986
0.996 123478-HxCDF
1.001 123678-KxCDF
1.005
1.019 234678-HxCDF
1.025
1.035
1.043 123789-HxCOF
1.047
1.050
1.053
1.056
1.059
1.064
859-1.141
0.000
0.961
0.966
0.996 13C12-HXCDF 478
1.000 13C12-HXCDF 678
1.011
1.018 13C12-HXCDF 234
1.043 13C12-HXCDF 789
1.052
AN
ZS3
AN
AN
AN
AN
SUR3
IS4
ALT2
ALT1
12,160.28
Above: HxCDF / HxCDD Follows
Triangle Laboratories, Inc.® Analytical Services Division
801 Capitola Drive • Durham, North Carolina 27713
Phone: (919) 544-5729 • Fax: (919) 544-5491
Printed: 14:55 09/11/97
45
-------
Page No.
09/11/97
Listing of S975807B.dbf
Matched GC Peaks / Ratio / Ret. Tiae
Conpound/
M_Z QC.Log Omit Why .-RT. OK Ratio Total.Area... Area.Peak.1.. Area.Peak.3.. Rel.RT Corapound.Name.. ID.. Flaga.
HXCDD
390-392
D
D
390-392
13C12-HXCDD
402-404
402-404
HpCDF
408-410
M
408-410
13C12- HpCDF
418-420
418-420
DC
DC
DC
DC
DC
DC
DC
DC
D
DC
D
DC
DC
DC
DC
DC
DC
DC
DC
DC
DC
DC
DC
DC
NL
SN
SN
SN
SN
SN
SN
SN
SN
SN
SN
SN
SN
WH
2
NL
SN
SN
6
NL
SN
SN
SN
WH
WH
4
NL
2
0:00
27:48
27:55
28 : 00
28:23
38:28
28:36
28:45
38:59
29:08
29:12
29:23
29:30
29 : 37
29:39
29:52
Peaks
0:00
28:35
28:53
29:06
29:12
29:29
29:39
29:43
29:48
Peaks
0:00
31:11
31:25
31:31
31:41
31:51
32:03
32:24
32:43
32:52
Peaks
0:00
31:11
32:23
Peaks
1.
RO
RO
RO
RO
RO
RO
RO
RO
RO
RO
1.
RO
RO
0.
RO
RO
RO
RO
RO
RO
RO
0.
RO
05-1.43
1
0
1
1
1
3
0
1
3
0
0
5
1
1
1
0
05
1
1
0
1
1
1
1
0
1
.34
.68
.23
.02
.08
.23
.88
.41
.64
.44
.90
.21
.13
.11
.66
.78
-1.43
.11
.06
.30
.21
.22
.24
.21
.89
.10
1.
1.
4.
0.
26.
2.
12.
0.
2.
1.
5.
0.
9.
3.
4.
2.
39.
94
63
12
79
87 13.95
37
36 6.84
99
04
30
40
65
23
55
12
62
23
0.951-1.015
12.92
7.80
0.000
0.952
0.956
0.959
0.971
0.975
0.979
0.985
0.993
0.998 123478-HxCDD
1.000 123678-HXCDD
1.006
1.010 123 789- HxCDD
1.014
1.015
1.033
AN
AN
AN
0.966-1.034
4.
14.
1.
2,038.
2,545.
2,932.
3.
6.
7.
7,544.
88-1.20
16
0
1
1
0
8
1
1
2
3
.57
.96
.02
.08
.70
.22
.49
.30
.70
.88
0.
31.
7.
8.
1.
0.
1.
6.
1.
0.
53.
32
32 7.37
32
12 1,115.09
55 1,400.67
97 1,622.47
76
39 3.54
09 3.71
44
1 / HpCDF Follows --
14
12 15 . 23
91 4.00
66 4.49
10
47
04
04 3.84
08
86
73
37-0.51
0
0
0
.60
.44
.43
1.
2,053.
1,189.
3,243.
83
55 627.33
64 360.12
19
6.95
933.03
1,144.88
1,310.50
3.97
3.38
0.
15.89
3.91
4.17
2.96
0.
1,436.23
839.53
0.000
0.979
0.989
0.997 13C12- HXCDD 478
1.000 13C12-HXCDD 678
1.010 13C12-HXCDD 789
1.015
1.018
1.031
995-1.045
0.000
1.000 1234678-HpCDF
1.007
1.011
1.016
1.021
1.028
1.039 1234789-KpCDF
1.049
1.054
936-1.128
0.000
1.000 13C12-HpCDF 678
1.038 13C12-HpCDF 789
SUR4
ISS
RS2
AN
AN
IS6
SOUS
Triangle Laboratories, Inc.® Analytical Services Division
801 Capitola Drive • Durham, North Carolina 27713
Phone: (919) 544-5729 • Fax: (919) 544-5491
Printed: 14:55 09/1 1/97
46
-------
Page Ho.
09/11/97
Listing of s975807B.dbf
Matched GC Peaks / Ratio / Ret.
Time
Compound/
M_z.... QC.Log Omit why ..RT. OK Ratio Total.Area... Area.Peak.1.. Area.Peak.2.. Rel.RT Compound.Name.. ID.. Flag*.
HpCDD
424-426
424-426
13C12-HpCDD
436-438
436-438
OCDF
442-444
442-444
OCDD
458-460
458-460
13C12-OCDD
470-472
DC
DC
DC
DC
DC
DC
DC
DC
DC
DC
DC
DC
DC
DC
DC
DC
DC
DC
DC
DC
DC
DC
DC
DC
DC
DC
DC
DC
NL
SN
2
NL
2
NL
SN
SN
SN
SN
SN
SN
SN
SN
SN
SN
SN
SN
SN
SN
SN
SN
SN
SN
SN
SN
1
NL
SN
SN
1
NL
0
31
31
32
:00
:26
:44
:02
0.
RO
RO
RO
---- Aoove: npv.ur /
88-1.20
0
1
0
1
.19
.39
.29
.14
Peaks
0
31
32
:00
:26
:02
0.
0
9
0
16
25
.14
.24
.35
.10
.34
88-1.20
0
1
1
Peaks
0
31
31
31
31
32
32
32
32
32
33
33
33
33
34
34
34
34
34
35
35
35
:00
:11
:13
:20
:49
:04
:12
:19
:27
:59
:12
:37
:40
:49
:05
:23
:27
:39
:52
:00
:23
:46
0.
RO
RO
RO
RO
RO
RO
RO
RO
RO
RO
RO
RO
RO
RO
RO
RO
RO
RO
RO
RO
.90
.10
.06
3
6
1,916
1,922
.07
.35
.64
.99
»i y
76-1.02
0
0
0
0
0
1
1
0
0
3
4
0
0
0
0
1
0
1
0
0
0
1
.16
.81
.43
.60
.23
.93
.67
.71
.15
.88
.92
.92
.41
.74
.17
.61
.36
.03
.13
.58
.67
.13
Peak
0
34
34
34
:00
-.31
:51
:55
0.
RO
RO
RO
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
7
0
1
0
1
7
.15
.65
.28
.45
.28
.79
.85
.68
.23
.45
.23
.48
.38
.53
.53
.68
.49
.09
.38
.78
.76
.66
.09
76-1.02
1
0
0
0
.00
.60
.44
.09
Peak
0
34
:00
:31
0.
RO
0
5
0
0
5
.14
.52
.57
.36
.52
76-1.02
1
0
.50
.89
0
1,696
.11
.66
6.28
8.59
3.32
984.58
0.977-1.006
0.000
4.53 0.981
0.991
7.51 1.000 1234678-HpCDD
AN
0.969-1.031
0.000
3.03 0.981
932.06 1.000 13C12-HpCDD 678 1ST
Oeta-CDD and CDF Follows
3.86
3.75
0.884-1.116
0.000
0.903
0.904
0.908
0.922
0.929
0.933
0.936
0.940
0.956
0.962
0.974
0.975
0.980
0.987
0.996
0.998
004 OCDF
010
014
025
AN
2.60
797.67
1.036
0.884-1.116
0.000
4.33 1.000 OCDD
1.010
1.012
0.996-1.005
0.000
898.99 1.000 13C12-OCDD
AN
IS8
Triangle Ubofatories, Inc.® Analytical Services Division
801 Capitola Drive • Durham, North Carolina 27713
Phone: (919) 544-5729 • Fax: (919) 544-5491
Printed: 14:55 09/11/97
-------
Page No. 6 Liating of S975807B.dbf
09/11/97 Matched GC Peaka / Ratio / Ret. Time
Compound/
M_Z.... QC.Log Omit why ..RT. OK Ratio Total.Area— Area.Peak.1.. Area.Peak.2.. Rel.RT Compound.Name.. ID.. Flag*.
DC WH 34:53 RO 1.19 3.08 1.011
470-472 1 Peak 1,696.66
Column Description 'Why' Code Description QC Log Deac.
M_Z -Nominal Ion Masa(es) HL-Below Retention Tine Window A-Peak Added
..RT. -Retention Trie (ma-.sa) HH-Above Retention Time window X-Peak Kept
Rat.l -Ratio of M/M-2 Ions SH-Below Signal to Noise Level D-Peak Deleted
OK -RO-Ratio Outside Limits
-------
File:S975807 #1-848 AaqtlO-SEP-1997 20,29:28 EI+ Voltag* SIS 70S JR>jUe>35
303.9016 T:2 SSUB(256,30,-3.0) PKD(9,S,5,0.05\,140.0,1.00\,r,T) ExpiXPCffS
TRIANGLE LASS TtitiTLI M23 BLANK TLIt43057 IKT. TIME - 20:32
1004 A5.45E4
17:00 18.00 19:00 20:00 21:00
rile:S975807 tl-848 AcgslO-SEP-1997 20:29:28 XI* Voltage SIX 70S Hoimut286
305.8987 Ts2 BSUB(256,30,-3.0) PKH(9, 5,5,0.05\,1144.0,1.00\,r,T) XxptEPCOS
TRIANGLE LASS T
-------
•il»:S975807 #1-848 AcqtlO-SSP-1997 20i29i2B EH- Voltmym SIX 708 Moi»*:38
319.8965 7:2 BSOB(256,30, -3.0) PKD(7,5,3,0.051,152.0,1.00\,r,T) XxftXTCOS
TRIANGLE LASS TextiXLI H23 BLANK XLIf 43057 ZJKT. XZMK - 20,32
10 0\ (
A4.11E4
A5.09S3
80:
A3.06X4
19100 20100 211 00
fil»:S975807 tl-848 AcqtlO-SXP-1997 20:29t28 XI* Voltmym SIR 70S Mo±m»,37
321.8936 T:2 SSUB(256,30, -3.0) PKD(7,5,3,0.05\,148.0,1.00\,r,T) XxptXPCOS
TXIAHGLX LASS Text!HI H23 BLANK TLH43057 UW. TDOS - 20:32
1001
Ai49*4 A7.04&7-3"3
Tllm:S975S07 tl-848 AcqtlO-SXP-1997 20:39:23 EI+ Voltage SIX 70S *>i*»*1012
331.9368 r:2 BSUB(256,30,-3.0) PXD(7,5,3,0.05\,4048.0,1.00\,T,T) XxptXPCDS
TRIANGLE LABS Text:TLI M23 BLANK TLIt43057 2X7. JDflT • 20:32
1001 A3.J.3X7
I
22 tOO
80-
60:
40:
20.
Al. 70X7
22 tOO
19:00 20,00 21:00
rilesS975807 tl-848 AcqtlO-SEP-1997 20,29:28 XI* Volt*g» SIX 70S 9o±**t42
333.9338 Tt2 BSUB(256,30,-3.0) PXD(7,5,3,0.05\,168.0,1.00\,r,T) XxpiXPCOS
TRIANGLE LABS TextiZZJ H23 BLANK TLH43057 HKT. T3XX - 20:32
100).
80:
60:
40:
20:
A3.18X7
22 tOO
19:00 20,00 21:00
File:S975807 #1-848 AcqtlO-SEP-1997 20,29,28 XH- Voltaya 5X2 70S Hoim»t34
327.8847 T:2 BSUB(256, 30, -3. 0) PKD( 7,5, 3, 0.05\,136.0,1.00\,TrT) XxptXPCOS
TRIANGLE LABS Text-.Til M23 BLANK TLH43057 TK7. TTHX • 20:32
10 OS A3 22X7
80:
60:
40:
20:
19:00 20,00 21:00
rilatS975807 tl-848 AcqtlO-SXP-1997 20:29:28 EH- Voltaye SIX 70S
330.9792 r,2 XxptXPCOS
TXIANSLS LABS T«Xt:TLI M23 BLANK TLIt43057 OtJ. XZMT
22,00
80:
60:
40:
20:
.5.6X6
-.4.5X6
13.4X6
.2.3X6
.1.1X6
ifl.oro
Tim.
.7.0X6
.5.6X6
.4.2X6
.3. 8X6
.1.4X6
O.OEO
7.7X6
6.2X6
4.6X6
3.1X6
1.5X6
0.0X0
Time
.5.5X6
.4.4X6
.3.3X6
.2.2X6
.1.1X6
.0. 0X0
19100
20:00
31,00
32100
50
-------
Tile,S975807 tl-848 AcgtlO-SEP-1997 20t29t28 EI+ Voltmgm SIX 70S Holme 139
339.8597 T:2 BSVB(2S6,30,-3.0) PKD(7, 5,3,0.05\, 156.0,1.00\,f,T) XxptSPCOS
TRIANGLE LASS Text:III H23 BLANK TLH43057 IHJ. HUB - 20,32
A3.90X4 A1.75X4
Al. 08X
23t00 24,00 25,00 26,00
ril»iS975807 91-848 AcqilO-SET-1997 20,29,28 EI+ VoltMye SI* 70S Holme,44
341.8567 Fi2 BSVB(256,30,-3.0) PKD(7,5,3,0.05\,176.0,1.00\,r,T) XxptXTCOS
TRIANGLE LABS Text.-TIT K23 BLANK TLH43057 IKJ. TZMK " 20,32
100\ A3.44X4
Time
26100
23',00 24,00 25,00
ril«:S975807 tl-848 AoqilO-SXP-1997 20,29,28 11+ Voltaya SIX 70S Ko±f»,38
351.9000 Tt2 BSUB(256,30,-3.0) PXD(7,5,3,0.05\,lS2.0,1.00\,r,T) KxptXPCOS
TRIANGLE LABS TtuctsTLI H23 BLANK TLIt430S7 ISJ. TIHX - 20,32
1003
80:
60:
40:
20:
0.
A2. 79X7
26,00
23:00 24100 25,00
F±l»iS975807 #1-848 Acq,10-SEP-1997 20:29,28 EI+ Voltagm SIX 70S Xoiae,39
353.8970 r,2 BSOB(256,30,-3.0) PKD(7,5,3, 0.05\, 156.0,1.00\,T,T) ExpiEPCDS
TRIANGLE LABS Text:3X1 H23 BLAKK TLIH3057 HIT. TIMS - 20,32
1001
80:
60:
40:
20:
o.
Al. 74X7
23100 24:00 25tOO 26:00
Fila:S975807 tl-848 AcqilO-SXf-1997 20:29:28 EI+ Volt*ga SIS 70S
330.9792 r:2 ExptEPCUS
TRIANGLE LABS Texts TLX M33 BUOtK TLIt430S7 TKT. TIHX " 20,32
100A 33,26 23^47 ^>J^. .. 35_,2J>_ 25,39 26,02
'. . .^^-^A^vv^
BO:
60:
40:
20:
o:
26:25
26100
23:00 24:00 25,00
Filt:S975807 fl-848 Acq:10-SEP-1997 20:39:28 EH- Volt*g» SIX 70S
409.7974 Ti2 Exp:XPCUS
TRIANGLE LABS TuxttTLI H23 BLANK TLH43057 ZKT. TIME - 20,32
100* 24 35
80:
60:
40:
20:
0.
.6X6
.9X6
.2X6
.4X6
.7X6
.0X0
Time
,0X6
,8X6
.6X6
,4X6
,2X6
,0X0
Time
,4X6
,2X6
.9X6
.6X6
.3X6
.0X0
time
23:00
24,00
25:00
26100
51
-------
'il»>S975807 #1-840 Acqi iO-SEr-L99/ 20t29t28 EI+ VoJ.t*ff* SIX 70S MOJH0I4J.
55.8546 F:2 BSOB(256,30,-3.0) PO>(7, 5,3,0. 05\,164 .0,1. 00\,r,T) XxpiXPCffS
TRIANGLE LABS Text. HI M23 BIAS* XLII430S7 HOT. TXMX " 20i32
IOCS
80J
40.
24:00 25i00 26.00
•ile.SS75807 #1-848 Acq,10-SEP-1997 20,29,28 EI+ Voltage SIX 70S Holme,36
357.8516 Tt2 BSOB(256,30,-3.0) PXD(7r5,3,0.05\r144.0,1.00\fr,T) XrptXPCUS
TSIAJKLX LABS TexttTLI H23 KURT TLH43057 XJK7. TIME -
1004 A6.24E4
A7.
3Z4
A7.34X4
A4.92E4
A1.97X4
[\A4.8BE3
J\M V Aw^.
Al. 09E4
A J\
-J.JI4
12.724
'-2.0E4
'.1.3X4
.6.7X3
'-0.0X0
TlmtA
24', 00 25,00 26,00
rile,S975807 fl-848 AoqilO-SXT-1997 30,29,28 EH- Voltage SIS 70S BoimetSS
367.8949 r»2 BSUB(256,30,-3.0) fB3(7,5,3,0.05\,140.0,1.00\rT,T) XacpiXPCOS
TRIANGLE LASS TexttTLI M23 KJUOC TLH43057 OKT. TXMX - 20,32
1003k A1.71X7
80.
60.
40.
20.
.68X6
24:00 25,00 26iOO
FilesS975807 tl-648 AcqtlO-SXP-1997 20i29t28 EH- Voltaga SIX 705 Jtoi*«»J4
369.8919 r:2 BSUB(2S6,30, -3. 0) KD(7,5,3,0.05\,136.0,1.00\,r,T) XxptXPCDS
TSIASGLX LABS TATtiTLI M23 BUOOC XLIt43057 HKT. TIKE - 20,32
100* A1.12X7
80.
60.
40.
20J
.07X6
24i00 25iOO 36tOO
rllftS975807 41-848 AcqilO-SXT-1997 20i29i28 EI+ VoltMff* SIX 70S
330.9792 Fi2 XxpiXPCOS
TSIANGLE LABS TexttTLI H23 MJOOC TLH43057 1ST. TIME • 20,32
10 0\
60.
40.
20.
0.
24146
26102
6,37
0.0X0
6.0X6
4.8X6
.3.6X6
.2.4X6
.1.2X6
.0.0X0
Time
.4.0X6
.3.2X6
.2.4X6
.1. 6X6
.8.1X5
0.0X0
Time
6.4X6
5.2X6
3.9X6
2.6X6
1.3X6
.0.0X0
24100
25100
26,00
J w
52
-------
File*S575S07 #1-405 AcqslO-SEP-1997 20t29i28 EH- Volttgm SIX 70S Hoim»>101»
373.8208 F:3 BSUB(25S, 30,-3.0) PKD(7,5,3, 0.05\,4072.0,1.00\,r,T) ExpiEPCUS
TRIANGLE LASS Text:TLI K23 BLANK XZI*43057 IJKT. TIME - 20:32
1001 Al.fOES
27:24 27.36 27.48 28.00 28.12 28.24 28.36 28.48 29.00 29.12 29.24 29.36 29.48 30.00 30.12
rile:S975807 #1-405 Acg-«10-S£P-1957 20.29.28 EH- Voltay* SIX 70S JR>l*«t5Jl
375.8178 F,3 BSUB(256,30,-3.0) PKD(7,5,3,0.05\,2124.0,1.00\,F,T) XzptXTCUS
TRIANGLE LABS TeitsTLI M23 BLANK TLH430S7 IK7. TIME - 20:32
Al. 43E5 -4.
ore
T±M»
27:24 27.35 27:48 28.00 28.12 28*24 28.36 28*48 29.00 29.12 29.24 29.36 25.48 30:00 30.12
Tila:S975807 #1-405 Ac?:10-SEF-1997 20129,28 EH- Volt*ya SIX 70S Holm*1772
383.8639 F:3 SSUB(256,30,-3.0) PXD(7r5,3,0.05\,3088.0r1.00\rr,T) XzpiEPCUS
TRIANGLE LABS Tezt.ZLX M23 BLANK TLH43057 1X7. TIME - 20.32
10 0\ Al.
BO.
sol
401
20:
0.
A7.65E6
27:24 27:35 27:48 28.00 28:12 28.24 28.35 28*48 25*00 29*12 29*24 25.35 25*48 30.00 30:12
rile.SS75807 #1-405 AcqslO-SEP-1997 20:29:28 EI+ Voltage SIX 70S Ooit»sl372
385.8610 F:3 BSUB(256,30r-3.0) PKU(7,5,3,0.05\,548e.O,1.00\,F,T) XifttfCOS
TSIANGLE LABS Text*2X1 M23 BLANK HI#43057 ZK7. TIME - 20*32
1001
80:
50:
40:
20:
o:
A1.54I7
27:24 27:35 27:48 28iOO 28:12 28<24 28<35 28:48 25:00 29:12 25:24 25:35 25:48 30:00 30112
rile:S975B07 #1-405 Acq:10-SEP-1997 20:25:28 EI+ Voltage SIX 70S
392.9760 T:3 ExptEPCDS
TRIANGLE LABS TextsIXJ M23 BLANK TLH43057 IJKT. TIME ' 20:32
27:25 -, ., 28.-1828.-2S 28:45 28:58
' •"-•"« ..*.*.... . 29sl3 29:25 25:40
5*6
7X6
4X5
.0X0
Tim*
.3X6
.6X6
.0X6
.3X6
.7X6
.0X0
1001
80:
50:
40:
20:
o:
30:07
27:24 27:36 27:48 28:00 28:12 28:24 28:36 2»»48 29f00 29:12 29:24 25iJ6'25:48'30« 00' 30.12
ril»sS975807 #1-405 AcqtlO-SEP-1997 20.25:28 EH- Voltage SIX 70S
445.7555 F:3 EiptEPCOS
TXIANGLE LABS TexttTLI M23 BLANK TLH43057 XKT. TIME " 20.32
8X6
2X6
7X6
1X6
5X5
0X0
Time
: 27:32 I 28.04
:-^v.—^_-AA->>*juu\-/iLi—«/A_^Au_.
27.24
53
-------
'i.lmtS975BQ7 tl-405 AcqtlO-SEP-J.997 2Ol2St2t SI* Voltag* SIX 70S Jtplt*i554
389.8156 Ts3 BSUB(256,30, -3.0) PKD(7,5,3,0.OS\,2216.0,1.00\,r,T) EzptEPCOS
TRIANGLE LABS T«xt.-IXI M23 BLANK TLX443057 IJCT. TIMX " 30>32
1001 A1.39X5
00:
so:
40.
27': 4 8 28:00 38,13 28:24 28,36 28,48 29,00 29,12 29,24
Tile.S575807 tl-405 AcqtlO-SEP-1997 20,29,28 EI+ Voltig* SIX 70S Noif 9,416
391.8127 r,3 BSOB(256,30,-3.0) PKD(7,5,3,0.05\, 1664.0,1.00\,r,T) XxptXPCUS
TRIANGLE LABS TfexttXCX M23 BLANK TLH43057 XK7. TIMS - 20,32
1001 A1.29E5
27,48 28,00 28,12 28,24 38,36 28,48 29,00 29,12 29,24 29,36
r±l»,S975807 #1-405 Acq:10-SEP-1997 30,39,38 EH- Voitmgm SIX 70S Hoi**, 1135
401.8558 f,3 BSVB(2S6,30,-3.0) PKD(7,5f 3,0.05\,4540.0,1.00\,r,T) XxptXfCOS
TRIANGLE LABS Text i HI M23 BLANK TLI443057 IKT. TIMX - 20,32
1001 A1.62X7
A3.31X4 A3.99X4
A4.90X4
6.3X4
5.024
3.814
2.5X4
1.3X4
29,36 29,48
29,48
ao:
60.
40.
20.
A1.40E7
27:48 28,00 28,12 28,24 28,36 28,48 29,00 29,12 29,24
File,S975807 H-405 A
-------
FilesS975807 tl-430 Acg:10-SEP-1997 20:29:28 EI+ Voltage SIS 70S Koif 9:581
407.7818 r:4 BSUB(256, 30, -3.0) PKD(7r5r3,0.05\r2324.0,1.00\,rfT) ExptEPCOS
TRIANGLE LABS T*Xt:TLI M23 BLANK TLIt43057 IJKT. TIME - 20*32
1001 A1.52E5
sol
60:
40:
20:
\
\ \ A4.49E4 A5.96E4
J y^ ^/^Vv/^V^ /v_^s5£L_^\4/^ /W-N^/^VA.
31:12 3l':24 31»35 31\48 32:00 32:12 32:24
rll»:S975807 tl-430 AcqtlO-SEP-1997 20:29:28 EH- Voltmgm SIX 70S Noia»:33
409.7789 T:4 BSDB(256,30,-3.0) PKD(7 ,5,3,0 .05\, 132. 0,1. 00\,t, T) Exp:EPCOS
TRIANGLE LABS Text : TL I M23 BLANK TLH43057 XKT. TIME - 20:32
1003
80:
60:
40:
20:
A1.59E5
l\
j 1 A4.17E4
\ I A3.91E4 A A3. 02X4
^ 1 V y*C/\Kdt-_ . , _ . _ . A. „
31:12 31:24 31:36 31:48 32:00 32:12 32:24
r±le:S975807 tl-430 Acq:10-SEP-1997 20:29:28 11+ Voltaov SIS 70S Noiac:379
417.8253 T:4 BSUB(2Sf,30,-3.0) PKD(7,5 ,3 ,0 .05\,1516.0,1. 00\,T,T) XxptEPCUS
TRIANGLE LABS T»xt:TLI M23 BLANK TLIt43057 IJKT. TIME - 20:32
1001
sol
60:
40:
20:
o:
A6.27E6
A
A
f \ A3. 60X6
A
/ \ /V
j v y v
31\12 31\24 3l':36 31\48 32\00 32*1,2 32:24
rile:S975807 tl-430 AcqtlO-SEP-1997 20:29:28 EH- Voltaga SIS 70S HOiae:635
419.8220 F:4 BSUB(256,30,-3.0) PKD(7,5,3,O.OS\,2540.0,1.00\,rrT) ExptEPCUS
TRIANGLE LABS TextsTLI M23 BLANK TLH430S7 HKT. TIME - 20:32
1001
80:
60:
40.
20:
o:
A1.43E7
A
A
I ! A8.30E6
A
/ \ /V
y v J ^
31:12 ' 31*24 ' ' 31:35 ' ' '31:48' ' ' 33\00 ' ' '32:12' ' '32:24'
TilesS975807 tl-430 AcqslO-SEP-1997 20:39:28 EH- Voltage SIR 70S
430.9729 T:4 Exp:EPCUS
TX I ANGLE LABS Text:TLI M23 BLANK TLH43057 UKT. TIME - 20:32
lOOi
ao:
60:
40:
201
ol
32:15 32:25
J**JU i r*~* J^ xv ^^^"^\y^ — ^^^\, .^-1,^-h
/ — ^s*^^~ — v — *^ — \A/" — ^ — ^~ \_ .^~^^~^-^ ^\/ ^
31:12 3l':24 31:36' ' ' 3l'i48 ' ' ' 32\6o' ' '32:12' ' 32:24
F11»>S975807 tl-430 Acq:10-SEP-1997 20:29:28 EI+ Voltag* SIS 70S
479.7165 Ts4 Exp:EPCDS
TRIANGLE LABS TexttZCX H23 BLANK TLIt43057 IJKT. TIME - 20:32
1003
so:
ffo:
40'
"
20.
o:
32:19
A , , 31i35
fi, „. ,..,, 31,26 A
sSti\\^-^SV\^J\^^\l\A~I\31'49 AAAJV\ All
31:12 31:24 31:36' ' '31:48' ' ' 32\0o' ' '32:12' ' ' 32\24
A1.43E4
.5.8E4
.4.7X4
.3.5X4
.3.3X4
J..2E4
.0 . 0*0
32:36' 32t^8 Tim*
» A5.35E3
.4.6X4
.3.7X4
.3.8X4
.1.9X4
.9.3E3
-0.0X0
32:36 32\48 t±M»
^3.3X6
.1 . 8X6
.1.4X6
.9.2X5
.4.6X5
0.0X0
32:36 32:48 Tif»
-5.3X6
.4.2X6
.3.2X6
.2.1X6
.1.1X6
0 . 0X0
32:36 32:48 Time
32:35 32:44 ir3'7E6
s~l^\r^s+. y^^*^ -J
•^ V^ ^ ^^^r ^•^ >r
'•.2.1X6
.1 . 6X6
.1 . 1X6
'.5.3X5
• o.oxo
32:36 32:48 Tim*
C2.0X4
32:37 32:41
J\.^y\.^~^J^.^-/ r
-1.6X4
.1.2X4
.8.2X3
.4.1X3
a. on)
32:36' ' ' 32t48 ' Tim9
55
-------
'ile:S975807 *I-4J0 Acqi 10-SEP-1S97 JOljytJB SI+ Voltage SIM 70S tfOl*eU6
423.7766 T>4 BSUB(256,30,-3.0) PKD(7,5,3,0.05\,144.0,1.00\,r,T) XxpiXPCUS
TXIANGLE LABS TexttTLI M23 BLANK TLH43057 ZK7. TIMX - 20:32
1001 AS 53X4
31:18 31:24 31:30 31:35 31:42 31:48 31:54 32:00 32:05 32:12 32:18 32:24
ril*iS975807 tl-430 AcqslO-SEP-1997 20:25:20 EI+ Voltage SIX 70S Boiset185
425.7737 F:4 BSUB(256,30,-3.0) PKD( 7,5,3, 0.05\,740.0,1.00\,r,T) XxpiXPCUS
TXIANGLE LABS TexttTLI M23 BLANK 111*43057 OUT. TIME * 20:32
1001 AT. 50X4
80:
50:
40:
20.
A 5.28X4
Al . 75E4
6.46E3
J\
^~^^^ ^S VN_
-3.1X4
12.5X4
'.1.9X4
-1.2X4
.5.2X3
32:3(>
,0.0X0
Tim<
so:
60'.
40:
A4.53E4
A6.2SS3
A5.40E3
^¥
A6.64E3
*&
A4.47X3
wJU
_2.7X4
.2.2X4
.1. 5X4
.1.1X4
.5.5X3
31:18 31:24 31:30 31:35 31:42 31:40 31:54 32i00 32:05 32<12 32:18 32:24 32:30 Time
r±leiS975807 tl-430 AcqtlO-SXP-1997 20:25:20 EI+ Voltage SIX 70S Soi»ei723
435.8169 Tt4 BSUB(256,30,-3.0) PKD(7,5,3, 0.05\,2892.0,1.00\,T,T) XxpiXTCOS
TXIANGLE LABS TejctiTLI M23 BLANK TLH43057 UKT. TIMX - 20:32
,00\ AS. 85X6 3.5X5
80. M '.2.8X6
60. I \ .2.1X6
40. I \ .1.4X5
20. / \ .7.1X5
31:24 31:30 31:35 31:42 31:40 31:54 32:00 32:05
rile>S97S807 tl-430 AcqtlO-SEP-1997 20:25:28 EH- Voltage SIX 70S Noi*e>811
437.8140 F>4 SSVB(256,30,-3.0) PKD(7,5,3, 0.05%,3244.0,1.00%,X,T> XxpiXPCUS
TXIANGLX LABS TexttTLI H23 BLANK TLIt43057 UfJ. TIME - 20:32
1001 A5.32X5
so:
50.
40.
20.
3224 3230
0.0X0
Tim,
.3.4X5
.2.7X6
.2.0X6
.1.4X6
.6.8X5
31:18 31:24 31:30 31:35 31:42 31:48 31:54 32:00 32:05 32:12 32:10 32:24
riletS975807 tl-430 AcqslO-SEP-1997 20:25:28 EI+ Voltage SIX 70S
430.9729 T:4 XxpiXPCOS
TXIANGLE LABS TexttTLI M23 BLANK TLIt43057 OfT. TIMS - 20:32
100* ,, ...
31:21 ":30
JV ~
00:
50:
40:
20.
32:30
0.0X0
Tim
.2.5X5
12.0X5
.1.5X5
.1.0X5
15.1X5
3li30
3li42 3li48 3liS4 32 32t06
3218 32, 24 3 2, 30
,0.0X0
Timel
J L
-------
Til»tS975807 #1-430 AcqslO-SEP-1997 20:29:28 XI+ Volt&gm SIX 708 Noif»t33
441.7428 F,4 SSOS(256,30, -3.0) PKO(7,5,3,0.05\,132.0,l.OO\,r,T) ExptSPCUS
TRIANGLE LASS TeztiXLI H23 BLANK TLH43057 1X7. TU€X • 20s32
1001
901
31tOO J2:00 JJtOO 34i00
TiletS97S807 tl-430 AcqilO-SEP-1997 20,29,38 EI+ Voltaya 5JX 70S Jfoi*«r217
443.7399 T:4 BSOB(256,30, -3.0) PKD(7,5,3,0.05\,86S.O,1.00\,T,T) ExpsEPCUS
TSIANSLE LASS TexttTLI M23 BLANK TLIf43057 UiJ. TIME - 30,32
10 0\
35:00
1.714
31:00 32tOO 33:00 34tOO
rilftS975807 #1-430 AcqslO-SEP-1997 20i29t28 EI+ Volttg* SIS 70S
430.9729 T:4 EipiEPCUS
TRIANGLE LASS ToxttXLI H23 SLAm TLH43057 U&. TUB -
35s 00
31:00 32:00 33:00 34,00
TilasS975B07 #1-430 AcqslO-SEP-1997 20:29:28 EH- Voltage SIS 70S
513.6775 f:4 EipsEPCOS
TXIANSLE LASS Text-.TLI H23 SLANK TLI#43057 HKT. TIXS « 20:32
34 23
35100
31:00
32:00
33:00
34:00
35:00
57
-------
•1J.*:S975B07 il-430 AcqtlO-SEP-1997 20t29,2B EI+ VoJ.t*gm SIM 70S
457.7377 r,4 BSUB(256,30,-3.0) PKD(7,5r3,0.051,144.0,1.00\,T,T> XxptXTCOa
TRIANGLE LABS TejtttXZI M23 BLANK TLIM3057 IXT. tlMX - 20}32
1001 A3.97E4
34154
34',24 34,30 34,36 34,42 34,48
til»tS975807 tl-430 AcqtlO-SXP-1997 20,29:28 XI* Vbltag* SIS 70S K>if»i43
469.7779 r>4 BSOS(25f, 30,-3.0) PR)( 7,5, 3,0.05\,172.0, L.OO\,T,T) Kip iff COS
TXIANGLZ LABS Taxt.Ttr H23 BLANK TLH43057 XK7. TIMS - 20,32
a 001 A7.98S6
-JL.3E4
34154
34124 34:30 34:36 34:42 34:48
ril0>S975807 il-430 AcqilO-SEP-1997 20:29:28 EI+ Voltajra SJJt 70S Hoim*>35
459.7348 f:4 BSVB(256,30,-3.0) PKD( 7,5, 3, 0. 05%, 140.0,1.00\,r,T) SxptftCOS
TRIANGLE LABS TfXtiTLI M23 BLANK TLH43057 IXT. TIMS - 20:32
1001 A4.
eo:
eo:
35tOO
40:
20:
.0.0X0
35 tOO Urn*
.2.0X6
11. 6X6
.1.2X6
.7.8X5
'.3.9X5
34:54
34:24 34:30 34:36 34:42 34:48
FilesS975807 tl-430 AcqslO-SEP-1997 20:29:28 EI+ Voltage SIS 70S Hoi**:28
471.7750 r>4 BSUB(2S6,30,-3.0) tKD(7,5,3, 0. 05\r 112.0,1.00\,r,T) XxptETCOS
TRIANGLE LABS Text:III H33 BLANK TLIM3057 ISJ. TIME • 20:32
.0.0X0
35 tOO Tim*
1001
>9S6
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-------
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-------
TLI Project: 43057 Method 23 TCDD/TCDF Analysis (DB-225)
Client Sample: TLI M23 Blank Analysis File: X973081
Client Project:
Sample Matrix:
TLI ID:
Sample Size:
Dry Weight:
GC Column:
A$FHfcr**r7.'J,'
XAD
TLI Blank
1.000
n/a
DB-225
Date Received:
Date Extracted:
Date Analyzed:
Dilution Factor
Blank File:
Analyst
II
09/06/97
09/11/97
n/a
S975807
MS
Spike File:
ICal:
ConCat
% Moisture:
% Lipid:
% Solids:
SPC2NF04
XF24087
X973069
n/a
n/a
n/a
2^,7,8-TCDF
0.005
'K:,2-2,3,7,8-TCDF
0.80
21:30
Data Reviewer
Page 1 of 1
09/12/97
C2NF_PSI»100. LARS 6.1004
Triangle Laboratories, Inc.*
801 Capitola Drive • Durham, North Carolina 27713
Phone: (919) 544-5729 • Fax: (919) 544-5491
Printed: 14:58 09/12/97
65
-------
Initial
..Date...
Data Review By:
/___ Calculated Noise Area: n/a
The Total Area for each peak with an ioa abundance ratio outside
ratio limit* has been recalculated according to Bet-hod requirement*.
Page No.
09/12/97
Listing of X973081B.dbf
Matched GC Peaks / Ratio
/ Ret. Tine
Compound/
M_Z QC.Log Omit Why ..RT. OK Ratio Total.Area... Area.Peak.1.. Area.Peak.3.. Rel.HT Compound.Ha»e.. ID.. Flags.
TCDF
304-306
304-306
DC
DC
DC
DC
DC
DC
DC
DC
DC
DC
DC
DC
DC
DC
DC
DC
DC
DC
DC
DC
DC
DC
DC
DC
DC
DC
DC
DC
DC
DC
DC
DC
DC
DC
DC
DC
DC
NL
SN
SN
SN
SN
SN
SN
SN
SN
SN
SN
SN
SN
SN
SN
SN
SH
SN
SH
SN
SN
SH
SN
SN
SN
SN
SN
SN
SN
SN
SN
SN
SN
SN
SN
WH
WH
4
0:
18:
18:
18:
18:
18:
18:
18:
19:
19:
19:
00
13
20
25
31
37
41
55
06
20
32
19:47
20:
20:
20:
06
16
20
20:24
20:33
20:42
20:
20:
21:
21:
21:
21:
21:
21:
21:
21:
22:
22:
22:
23:
23:
23:
23:
24:
24:
24:
24:
24:
25:
49
54
13
20
28
32
36
46
53
56
03
25
32
10
13
34
51
18
28
36
40
58
01
0.
RO
RO
RO
RO
RO
RO
RO
RO
RO
RO
RO
RO
RO
RO
RO
RO
RO
RO
RO
RO
RO
RO
RO
RO
RO
RO
RO
RO
RO
RO
RO
RO
65-0.89
1
5
0
2
1
0
0
2
0
1
0
2
1
2
0
0
0
1
0
0
0
3
1
0
0
0
0
0
2
0
0
2
0
0
0
0
1
0
3
1
0
.76
.21
.84
.53
.04
.56
.79
.07
.73
.23
.87
.52
.92
.13
.61
.57
.33
.39
.65
.36
.76
.46
.31
.48
.27
.38
.85
.07
.73
.60
.83
.16
.20
.60
.57
.40
.64
.43
.60
.94
.68
Peaks
3.
1.
7.
0.
5.
1.
9.
5.
57.
6.
6.
13.
15.
18.
4.
6.
3.
6.
19.
3.
27.
1.
8.
8.
3.
2.
6.
0.
2.
9.
27.
3.
1.
7.
2.
1.
2.
7.
1.
1.
4.
130.
54
49
42
60
82
20
48
61
04
05
89
45
35
23
80
11
10
62
28
59
16
50
66
92
03
99
44
87
99
47
80
98
59
42
74
26
55
79
19
38
02
23
24.05
21.97
11.70
12.60
0.797-
0.
0.
0.
0,
0.
0.
0.
0.
32.99 0.
0,
0.
0.
0.
10.30 0.
0,
0,
0.
0.
0.
0,
15.46 0.
0,
0,
0.
0.
0.
0,
0.
0.
0.
15.20 1.
1.
1.
1.
1.
1.
1.
1.
1.
1.
1.
1.100
000
809
814
818
822
827
830
840
848
859
868
879
893
900
903
906
913
919
925
928
942
947
9S3
956
959
967
972
974
979
996
001 2378-TCDF
029
031
047
059
079
087
093
095
109
111
AN
Triangle Laboratories, Inc.® Analytical Services Division
801 Capitola Drive • Durham, North Carolina 27713
Phone: (919) 544-5729 • Fax: (919) 544-5491
Printed: 14:58 09/1 2/97
66
-------
Page No. 2 Listing of X973081B.dbf
09/12/97 Matched GC Peaks / Ratio / Ret. Time
Compound/
M_Z.... QC.Log OBit Why ..RT. OK Ratio Total.Area... Area.Peak.1.. Area.Peak.2.. Rel.RT Compound.Name.. ID.. Flag*.
13C12-TCDF 0.65-0.89 0.955-1.045
316-318 DC ML 0:00 RO 1.24 8.04 "' 0.000
DC WL 21:11 RO 0.92 116.20 0.941
DC WL 21:26 0.76 140.82 0.952
1.000 13C12-2378-TCDF ISO
1.026
DC WH 24:31 0.66 263.74 1.089
316-318
WL 21:26
22:31
23:06
WH 24:31
2 Peaks
0.76
0.78
0.83
0.66
140.82
25,717.50
74.32
263.74
25,791.82
11,307.90
33.73
14,409.60
40.59
Above: TCDP / TCDD Follows
13C12-TCDD 0.65-0.89 0.906-1.094
332-334 DC NL 0:00 RO 2.13 6.73 0.000
.948
.000 13C12-2378-TCDO IS1
.013 13C12-1234-TCDD RSI
.044
DC WH 23:50 RO 0.40 35.47 1.122
332-334
NL 0:00 RO 2.13
20:08 RO 1.01
21:14 0.77
21:30 0.80
22:10 0.77
WH 23:50 RO 0.40
4 Peaks
6.73
97.12
20,642.36
25,442.00
267.84
35.47
46,449.32
55.52
8,983.46
11,298.80
116.93
0
54.87 0
11,658.90 1
14,143.20 1
150.91 1
1
Column Description 'Why* Code Description QC Log Desc.
M_Z -Nominal Ion Mass(es) HL-Bclow Retention Time Window A-Peak Added
..RT. -Retention Tiae (ma:as) WH-Above Retention Tiae Window K-Peak Kept
Rat.l -Ratio of M/M+2 Ions SN-Below Signal to Noise Level D-Peak Deleted
OK -RO-Ratio Outside Limits
-------
'11»:X9730B1 il-1285 Acqtll-sSP-1997 21,07:37 OC gl» Voltage SIX Autogp»a Soli»tl753
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18:00 19:00 20:00 21:00 22:00 23:00
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375.8364 Xxp:XCONP_TT
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100ft 10(10
24 tOO
10(00
20:00
21:00
22(00
23(00
24100
25 00
.2.8X7
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-------
'lla:X373081 91-1285 AC00 23tOO
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327.8847 BSUB(256,30,-3.0) PXD(S,3,l,0.10*,4308.0,0.00*fP,P) Exp:ICONS' TT
Saapl* TaxttTLI M23 BULKX TLI*43057 file Tnctt TRUNQLB LABS ~
100* U..7.9S8
80.
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A8.98E7
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24:00
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0.0X0
Timm
^2.3X7
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Tim*
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1
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69
-------
18:00 15:00 20:00 21:00 22:00 23:00
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15.5415 Xxp:ICOKP_TT
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PlleiX973081 #1-1285 Aeg:ll-SXP-1557 21:07:37 OC XT* Voltaff* SIR AutoSp.c
315.8565 Exp:KONP_TT
Sample TexttTLI K23 BLAH* TLHH3057 Pile Textt TSIAOOLX LABS
loan
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23:00
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70
-------
Peak Locate Examination:ll-SEP-1997:21:07 File:X973081
Experiment:XCONF_TT Function:! Reference:PFK
-------
File;X973081 #1-1285 Acq:ll-5Ep-1997 21;07;37 GC EI+ Voltage SIR AutoSpec
303.9016 Exp:XCONF_TT
Sample Text:TLI M23 BLANK TLI#43057 File Text: TRIANGLE LABS
100% A1.26E5
80.:
60J
40J
20J
OJ
22:0023:0024:00
File:X973081 #1-1285 Acq:ll-SEP-1997 21:07:37 GC EI+ Voltage SIR AutoSpec
305.8987 Exp:XCONF_TT
Sample Text:TLI M23 BLANK TLI#43057 File Text: TRIANGLE LABS
100%
80j
60 j
40J
20J
ol
ile:X973081 #1-1285 Acq:ll-SEP-1997 21:07:37 GC EI+ Voltage SIR AutoSpec
315.9419 Exp:XCONF_TT
Sample Text:TLI M23 BLANK TLI#43057 File Text: TRIANGLE LABS
100%
7.4E4
_5.9E4
_4.4E4
_3.0E4
_1.5E4
25:00
O.OEO
Time
22
•00
23
•00
24
loo
25
loo
Time
22:31
)\
22100 23100 24100 25:00
2.8E7
L2.2E7
_1.7E7
_5.6E6
0 OEO
Til
-------
FLI Project: 43057
:iient Sample: I-M23-1
Method 23 PCDD/PCDF Analysis (a)
Analysis File: S975808
Client Project: ASPECT Pi4/uT "ft"
Sample Matrix: M23TRAIN Date Received: 08/29/97
TLIID- 181-27-1A-C Date Extracted: 09/06/97
Date Analyzed: 09/10/97
Sample Size: 1.000
Dry Weight n/a
GC Column: DB-5
>'* ^ N. . *t~ 'b$fr.^.-
2,3,7,8-TCDD
1^3,7,8-PeCDD
1,23,4,7,8-HxCDD
1,2^,6,7,8-HxCDD
1,23,7,8,9-HxCDD
lA3,4,6,7,8-HpCDD
1,2,3,4,6,7,8,9-OCDD
2,3,7,8-TCDF
1,23,7,8-PeCDF
2,3,4,7,8-PeCDF
1,23,4,7,8-HxCDF
1,2^,6,7,8-HxCDF
2,3,4,6,7,8-HxCDF
1,2^,7,8,9-HxCDF
1,2^,4,6,7,8-HpCDF
1,23,4,7,8,9-HpCDF
1,2,3,4,6,7,8,9-OCDF
Dilution Factor n/a
Blank FUe: S975807
Analyst ML
o jUHfc'ftMft- "^^i^^giagiN^^^
EMPC 0.004
0.01
0.02
0.04
0.05
0.72
44.5
0.04
0.008
0.02
0.06
0.02
EMPC 0.02
0.007
0.12
0.04
0.16
Spike FUe:
ICal:
ConCal:
% Moisture:
%Lipid:
% Solids:
1.34
1.42
1.16
1.09
0.98
0.87
0.75
1.68
1.46
137
1.32
1.40
1.13
0.97
0.90
SPX23704
SF56117
S975797
n/a
n/a
n/a
25:52
29:08
29:13
29:30
32:04
34:33
20:26
24:44
25:30
28:23
28:29
29:42
31:11
32:24
34:39
^ _
PR!
-
B_
iZ
PRB
B
PRB
PRB
B_
B_
^i%^'>^^^1 A*«t && xlftwJ^^g^fpft' ^-^^l^^ ^^%%&$;
Total TCDD
Total PeCDD
Total HxCDD
Total HpCDD
Total TCDF
Total PeCDF
Total HxCDF
Total HpCDF
0.05 4 0.06
0.07 3 0.21
0.45 7
1.6 2
0.14 10 0.17
0.12 5 0.12
0.19 8 0.23
0.30 4
^ ^^
___
___
Page 1 of2
X237JSI «UO. LUtS 4.W.O4
Triangle Laboratories, Inc.*
801 Capitola Drive • Durham, North Carolina 27713
Phone: (919) 544-5729 • Fax: (919) 544-5491
Printed: 14:56 09/11/97
•--„•- 73
-------
TLI Project 43057
Client Sample: I-M23-1
Method 23 PCDD/PCDF Analysis (a)
Analysis File: S975808
13C,r-2,3.7,8-TCDF
l3C,r2,3.7,8-TCDD
I3C12-lA3,7,8-PeCDF
uC,2-lA3,6,7,8-HxCDF
13C,rl^3,6,7,8-HxCDD
"C,rl,2,3,4,6,7,8-HpCDF
13C,2-lA3,4,6,7,8-HpCDD
I3C ii-l ,2,3,4,6,7,8,9-OCDD
3.9
3.6
3.8
4.1
4.1
3.7
2.8
3.1
4.8
98.5
89.0
95.5
103
102
93.6
71.1
78.3
60.5
40%-130%
40%-130%
40%-130%
40%-130%
40%-130%
40%-130%
25%-130%
25%-130%
25%-130%
0.76
0.79
1.42
1.49
0.50
1.24
0.45
1.03
0.86
20:24
21:13
24:43
25:51
28:29
29:12
31:11
32:03
34:32
1JC,rZ3,4,7,8-PeCDF
l3Ca-lA3,4,7,8-HxCDF
uCirl,2,3,4,7,8-HxCDD
»C,rl,^3,4,7,8,9-HpCDF
3.9
3.7
3.8
3.5
97.6
93.2
94.6
88.0
83.6
70%-140%
70%-140%
70%-140%
70%-140%
70%-140%
1.45
0.50
1.20
0.41
21:14
25:29
28:22
29:07
32:23
13Cur2^,4,6,7,8-HxCDF
3.7
4.0
91.3
99.0
40%-130%
40%-130%
OJO
0.49
29:42
28:59
I3C12-U,3,7,8,9-HxCDD
0.80
21:01
29:29
Data Reviewer.
(V-
09/11/97
Page 2 of2
JO37J>S* .iDO, UJtS &KX04
Triangle Laboratories, Inc.®
801 Capitals Drive • Durham, North Carolina 27713
Phone: (919) 544-5729 - Fax: (919) 544-5491
Printed: 14:56 09/1 1/97
74
-------
Initial
Data Review By:
Calculated Noise Area:
2.89
The Total Area for each peak with an ion abundance ratio outside
ratio liaits has been recalculated according to method requirements.
Page No. 1 Listing
09/11/97 Hatched
Compound/
M_Z QC.Log Omit Why . .RT. OK
TCDF 0.
304-306
K
K
A
M
304-306
13C12-TCDF
316-318
316-318
TCDD
320-322
K
A
MK
H
DC NL 0
16
17
17
18
18
18
19
19
19
20
20
20
21
DC SN 21
22
:00
-.56
:23
:40
:04
:27
-.54
:14
:43
:58
:12
:26
:5S
:09
:43
:20
RO
RO
RO
RO
RO
of S975808B.dbf
GC Peaks / Ratio / Ret. Tine
Ratio Total. Area. . . Area. Peak.
65-0.89
0
0
0
0
0
0
0
0
0
0
0
0
0
1
0
0
.15
.75
.74
.73
.98
.81
.88
.68
.88
.71
.82
.75
.94
.07
.84
.95
14 Peaks
DC NL 0
DC WL 19
19
19
20
20
.-00
:12
:40
:55
:24
:54
0.
RO
RO
0.14
6.90
8.43
10.53
18.92
24.57
30.00
25.49
31.80
40.05
11.18
75.49
15.12
7.81
3.50
12.27
318.56
2
3
4
10
11
14
10
14
16
5
32
8
4
6
1. . Area. Peak.
.95
.58
.46
.47
.02
.00
.35
.90
.66
.05
.29
.07
.72
.59
3
4
6
10
13
16
15
16
23
6
43
8
4
6
,65-0.89
0
0
0
0
0
1
4 Peaks
DC NL 0
DC ML 18
18
18
19
DC SN 19
DC SN ISi
DC SN 19
19
DC SN 20
DC SN 20
20
21
:00
:10
:18
:45
:08
:19
:40
:46
:53
:05
:46
:57
:14
0.
RO
RO
RO
RO
RO
RO
RO
.75
.66
.66
.50
.76 6
.10
6
,65-0.89
0
0
0
0
0
0
0
0
0
1
0
0
0
.13
.58
.73
.66
.81
.71
.53
.23
.48
.33
.88
.86
.37
2.05
21.11
32.43
26.32
,033.07
22.87
, 114 . 69
TCDF /
0.16
0.80
27.69
15.97
6.74
0.82
1.36
0.46
12.96
3.56
1.05
10.21
5.63
12
11
2,601
14
.88
.45
.46
.24
19
23
3,431
12
2..
0.
.95
.85
.07
.59
.55
.00
.14
.90
.39
.13
.20
.54
.41
.93
0.
.55
.12
.61
.92
Rel.RT Compound. Haae. . ID.. Flag*,
823-1.104
0.000
0.830
0.852
0.666
0.886
0.904
0.926
0.943
0.967
0.979
0.990
1.002 2378 -TCDF AN
1.025
1.037
1.065
1.095
951-1.049
0.000
0.941
0.964
0.976
1.000 13C12-2378-TCOF ISO
1.025
11
6
3
5
4
2
.72
.36
.02
.64
.73
.45
15
9
3
11
5
6
0.
.97
.61
.72
.80
.48
.57
857-1.061
0.000
0.856
0.863
0.884
0.902
0.910
0.927
0.932
0.937
0.947
0.979
0.987
1.001 2378 -TCDD AH
Triangle Laboratories, Inc.® Analytical Services Division
801 Capitola Drive • Durham, North Carolina 27713
Phone: (919) 544-5729 • Fax: (919) 544-5491
Printed: 1456 09/11/97
:j j. 75
-------
Page No.
09/11/97
Hating of S97S808B.dbf
Matched GC Peaka / Ratio / Ret. Tiae
Compound/
M_Z QC.Log Omit Why ..RT. OK Ratio Total. Area. .. Area. Peak. 1.. Area. Peak. 2.. Rel.RT Compound. Name.. ID.. Flag*.
K
320-322
37C1-TCDD
328
328
13C12-TCDD
332-334
332-334
PeCDF
340-342
0
A
M
D
340-342
13C12- PeCDF
352-354
DC
DC
DC
DC
DC
DC
DC
DC
DC
DC
DC
DC
D
DC
DC
D
DC
DC
DC
DC
DC
SN
SN
WH
7
NL
WL
WL
3
ML
4
NL
SN
SN
SN
SN
SN
SN
SN
SN
SN
SN
SN
WH
6
NL
21:24
21:37
22:03
22:39
Peaka
0:00
18:36
18:45
19:41
21:14
21:42
Peaka
0:00
19:54
21:01
21:13
21:35
Peaka
0:00
22:29
22:37
22:55
23:42
23:49
24:00
24:09
24:21
24:38
24:44
24:53
25:04
25:30
25:57
26:21
26:28
26:38
26:55
Peaks
0:00
23:49
24:21
24:43
RO
RO
RO
RO
0.
RO
RO
1.
RO
RO
RO
RO
RO
RO
RO
RO
RO
1.
RO
0.
0.
0.
0.
14
47
29
59
18,
3,
21,
1
3
0
1
82
1
671
146
140
630
183
954
.63
.24
.90
.13
.44
.00
.91
.56
.50
.46
.22
.18
1.41
18,140.50
3,630.46
183 , 22
65-0.89
17.
0.
0.
0.
0.
57
94
80 4,
79 4,
76
9,
32-1.78
0.
1.
1.
0.
1.
1.
1.
1.
1.
1.
1.
1.
1.
1.
0.
1.
1.
0.
1.
32-
1.
1.
1.
1.
78
04
56
16
13
48
74
43
48
95
68
39
81
46
72
09
60
42
36
1.78
14
53
42
42 5,
0
20
648
411
69
.12
.87
.40
.05
.35
149.67
TCDD /
0
1
40
0
5
53
8
9
26
8
10
8
14
29
2
11
6
1
3
173
0
39
22
030
.12
.92
.44
.54
.05
.70
.97
.00
.50
.42
.65
.01
.13
.89
.73
.91
.22
.86
.82
.09
.13
.40
.55
.90
11.14
2,068.45
1,945.04
29.97
24.67
32.09
15.80
6.68
17.76
7.24
23.80
13.25
2,953.19
1.009
2.97 1.019
1.039
1.068
0.906-1.094
0.000
0.877
0.864
0.928
1.001 37C1-TCDD
1.023
0.906-1.094
0.000
11.79 0.938
2,579.95 0.991 13C12- 1234 -TCDD
2,466.01 1.000 13C12-2378-TCDD
39.38 1.017
0.909-1.079
0.000
0.910
15.77 0.915
0.927
0.959
21.61 0.964
0.971
0.977
10.70 0.985
0.997
3.97 1.001 12378-PeCDF
1.007
1.014
12.13 1.032 23478-PeCDF
1.050
6.64 1.066
1.071
1.078
1.089
0.838-1.162
0.000
15.60 0.964
9.30 0.985
2,077.71 1.000 13C12-PeCDP 123
STJR1
RSI
IS1
AH
AN
IS2
Triangle Laboratories, Inc.® Analytical Services Division
801 Capitola Drive • Durham, North Carolina 27713
Phone: (919) 544-5729 • Fax: (919) 544-5491
Printed: 14:56 09/1 1/97
76
-------
'age No.
J9/11/97
Listing of S975808B.dbf
Matched GC Peak* / Ratio / Ret. Tine
:ompound/
«_Z QC.Log Omit Why ..RT. OK Ratio Total.Area. ..
Area.Peak. 1.. Area.Peak.2.. Rel.RT Compound.Name.. ID.. Flags.
352-354
PeCDD
356-358
356-358
13C12- PeCDD
368-370
368-370
HxCDF
374-376
K
A
M
MK
H
25:02
25:29
DC SN 26:27
5 Peaks
DC NL 0
23
24
24
24
25
25
25
25
:00
-.58
:11
:27
:44
:04
:18
:32
:52
RO
1.
RO
RO
RO
RO
RO
RO
1.61
1.45
4.31
32-1.78
0.88
0.01
0.01
2.79
1.98
1.36
1.51
1.27
1.34
8 Peaks
DC NL 0
DC SN 24
DC SN 25
25
26
DC SN 26
26
:00
:47
:13
:51
-.00
:19
:51
1.
RO
RO
RO
RO
RO
3 Peaks
DC NL 0
27
27
27
28
28
28
28
28
28
28
DC SN 29
DC SN 29
DC SN 29
DC SN 29
DC SN 29
29
29
DC SN 29
DC WH 30
:00
:23
:32
:50
:00
:23
:29
:36
.•46
:57
:59
:07
:14
:24
:31
:38
:42
:48
:55
:02
1.
RO
RO
RO
RO
RO
RO
RO
RO
RO
RO
RO
32-1.78
1.00
0.62
0.82
1.49
1.52
0.73
0.32
05-1.43
1.30
1.52
1.37
1.24
1.29
1.37
1.32
1.22
1.24
0.99
1.86
1.45
3.90
0.57
11.93
7.38
1.40
1.61
3.55
0.73
34.52
4,547.45
8.26
9,674.82
: PeCDF /
0.12
55.24
18.79
24.15
22.29
18.58
38.84
8.69
9.59
196.17
21.28
2,691.90
13.
1,855.
33
11
26
17
10
23
5
5
.58
.42
.39
.28
.70
.37
.28
.50
4,006.
846.
9.
8.
7.
15.
4.
4.
24
55
1.013
1.031 13C12-PeCDF 234
1.070
SOR2
0.921-1.026
77
02
47
74
88
47
15
09
0.000
0.927
0.936
0.946
0.957
0.970
0.979
0.988
1.001 12378-PeCDD
AM
0.845-1.155
0.12
3.88
2.81
3,028.25
293.47
4.95
9.08
3,330.80
1,813
177
5
.06
.23
.52
1,215.
116.
17.
19
24
44
0.000
0.959
0.975
1.000 13C12- PeCDD 123
1.006
1.018
1.039
153
2.00
19.47
62.51
9.10
31.54
75.02
29.20
7.16
9.81
7.55
19.04
1.34
0.87
1,01
0.3J.
0.72
7.57
11.47
1.05
1.03
13
36
5
17
43
16
3
5
4
15
4
.20
.14
.04
.77
.35
.64
.93
.43
.18
.80
.42
8.24
8.
26.
4.
13.
31.
12.
3.
4.
4.
8.
3.
5.
0.957-1.053
69
37
06
77
67
56
23
38
23
50
,15
12
0.000
0.961
0.967
0.977
0.983
0.996 123478-BxCDF
1.000 123678-HxCDF
1.004
1.010
1.016
1.018 234 678 -HxCDF
1.022
1.026
1.032
1.036
1.040
1.043 123789-HXCDF
1.046
1.050
1.054
AM
AM
AN
AM
P*
PR
Triangle Laboratories, Inc.® Analytical Services Division
801 Capitola Drive • Durham, North Carolina 27713
Phone: (919) 544-5729 • Fax: (919) 544-5491
Printed: 14:56 09/11/97
77
-------
Page No.
09/11/97
Listing of s97S808B.dbf
Matched GC Peaks / Ratio / Ret. Time
Compound/
M_2 QC.Log Omit why ..RT. OK Ratio Total.Area... Area.Peak.1.. Area.Peak.2.. Rel.RT Compound.Same.. ID.. Flags
374-376
13012-HxCDF
384-386
384-386
BxCDD
390-393
390-393
13C12-HXCDD
402-404
DC WH 30:16 RO
12 Peaks
0.
DC NL 0:00 RO
DC SN 27 :
27:
28:
28:
DC SN 28 :
28:
DC SN 29 :
29:
DC SN 29 :
29:
23
31
22
29
46 RO
59
14 RO
23 RO
31 RO
42
1.47
43-0.59
0.98
0.
0.
0.
0.
1.
0.
0.
1.
0.
0.
6 Peaks
DC NL 0:
27:
28:
DC SN 28 :
28:
28:
DC SN 28 :
39:
29:
29:
DC WH 29:
1.
00 RO
55
23
28 RO
36
45
53 RO
08
13
30
41 RO
53
51
50
50
19
49
88
74
89
50
3.43
289.44
3.47
6.19
16.32
3,532.36
3,893.18
2.67
3,490.34
2.07
7.19
4.27
2,799.07
13,738.46
05-1.43
1.
56
1.22
1.29
3.38
1.19
1.18
0.75
1.42
1.16
1.09
0.85
7 Peaks
DC NL 0:
1.
00 RO
DC WL 27:53 RO
38:36
39:07
39:13
29:29
29:41
DC SH 29:48 RO
402-404
HpCDF
408-410
M
nxt-uc /
2.08
75.74
68.09
1.75
103.06
17.87
2.33
15.54
29.95
42.60
5.18
352.85
1.063
0.859-1.141
0.000
5.
1,175.
1,290.
1,154.
8.
931.
54
53
86
25
30
12
10.
2,356.
2,602.
2,336.
78
83
32
09
4.76
1,867.
95
0.961
0.966
0.996 13C12-HXCDF 478
1.000 13C12-HxCDF 678
1.010
1.018 13C12-KXCDF 234
1.026
1.032
1.036
1.043 13C12-HXCDF 789
SOR3
IS4
ALT2
ALT1
41.
38.
55.
9.
9.
16.
22.
58
41
90
67
,11
.07
.25
34
29
47
8
6
13
20
,05-1.43
0.82
0.66
1
1
1
1
1
2
5 Peaks
DC NL 0
31
31
31
DC SN 31
0
-.00 RO
:11
:24
:33
:51 RO
.23
.20
.24
.23
.36
.82
1.45
2.96
12.52
2,521.18
2,943.73
3,161.62
9.42
1.39
8,648.47
.88-1.20
1
1
1
1
0
.64
.13
.10
.03
.66
3.51
94.90
16.64
78.61
1.26
6
1,375
1,628
1,743
5
.91
.41
.34
.31
.42
5
1,145
1,315
1,418
4
0.951-1.015
.16
.68
.16
.20
.43
.88
.35
0.000
0.956
0.972
0.975
0.979
0.985
0.989
0.998 123478-HXCDD
1.001 123678-HxCDD
1.010 123789-HXCDD
1.017
AN
AN
AN
0.966-1.034
.61
.77
.39
.31
.00
0.000
0.954
0.979
0.997 13C12-HXCDD 478
1.000 13C12-HXCDD 678
1.010 13C12-KXCDD 789
1.017
1.021
SCR4
IS5
RS2
50
8
39
.40
.73
.83
44
7
38
0.995-1.045
.50
.91
.78
0.000
1.000 1234678-HpCDF
1.007
1.012
1.021
AN
PR
PR
Triangle Laboratories, Inc.® Analytical Services Division
801 Capitola Drive • Durham, North Carolina 27713
Phone: (919) 544-5729 • Fax: (919) 544-5491
Printed: 14-56 09/11/97
78
-------
•age No.
19/11/97
Liating of S975808B.dbf
Matched GC Peak* / Ratio / Ret. Time
:onpound/
<_Z QC.Log Omit Why ..RT. OK Ratio Total.Area... Area.Peak.1.. Area.Peak.2.. Rel.RT Compound.Name.. ID.. Flag*.
108-410
13C12-HpCDF
418-420
418-420
HpCDD
424-426
424-426
13C12-HpCDD
436-438
436-438
OCDF
442-444
442-444
DC
DC
DC
DC
DC
DC
DC
DC
DC
DC
DC
DC
DC
DC
DC
DC
DC
DC
DC
DC
DC
DC
DC
DC
DC
DC
SN
4
NL
2
ML
2
NL
1
NL
SN
SN
SN
SN
SN
SN
SN
SN
SN
SN
SN
SN
SN
SN
SN
SN
SN
SN
SN
SN
SN
1
31:
32:
58
24
RO
2.
0.
11
97
Peaks
0:
31:
32:
00
11
23
0.
RO
1.
21.
211.
65
27 10.45
42
37-0.51
0.
0.
0.
Peaks
0:
31:
32:
00
27
04
0.
RO
82
45
41
88-1.20
1.
0.
0.
74
96
98
Peaks
0:
32:
00
03
0.
RO
88-
1.
1.
Peak
0:
30:
31:
31:
31:
31:
32:
32:
32:
32:
32:
33:
33:
33:
33:
33:
33:
34:
34:
35:
35:
35:
35:
00
56
08
33
47
52
01
12
27
35
52
01
08
20
31
34
48
39
55
04
15
26
48
0.
RO
RO
RO
RO
RO
RO
RO
RO
RO
RO
RO
RO
RO
RO
RO
RO
RO
RO
76-
0.
3.
0.
7.
4.
0.
0.
1.
1.
0.
1.
0.
0.
2.
1.
0.
2.
0.
0.
0.
0.
1.
1.
1.20
22
03
1.02
86
00
36
31
29
52
38
04
41
23
16
97
13
16
15
58
41
90
80
35
85
53
05
Peak
2.
1,994.
1,285.
10
27 614.76
52 375.39
1
10.82 1
.025
.039 1234789-HpCDF
AN
0.936-1.128
0
1,379.51 1
910.13 1
.000
.000 13C12-HpCDr 678
.038 13C12- HpCDF 789
IS6
SOBS
3,279.79
HpCDF / HpCDD Follows ~ **
3.
463.
385.
849.
35
72 227.09
95 190.80
67
0.977-1.006
0
236.63 0
195.15 1
.000
.981
.001 1234678-HpCDD
AM
0.969-1.031
2.
2,016.
75
39 1,023.54
2,016.39
HpCDD / Octa-CDD and CDF
0.
0.
0.
0.
0.
0.
0.
0.
0.
0.
1.
1.
0.
1.
1.
0.
0.
59.
4.
1.
1.
1.
2.
59.
13
34
45
25
13
91
42
87
42
25
46
40
19
63
23
68
51
10 28.00
15
42
26
00
99
10
0
992.85 1
.000
.000 13C12-HPCDD 678
IS7
Follows ----------
0.884-1.116
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
31.10 1
1
1
1
1
1
.000
.896
.902
.914
.920
.923
.927
.932
.940
.944
.952
.956
.959
.965
.971
.972
.979
.003 OCDF
.011
.015
.021
.026
.037
AN
Triangle Laboratories, Inc.® Analytical Services Division
801 Capitola Drive • Durham, North Carolina 27713
Phone: (919) 544-5729 • Fax: (919) 544-5491
Printed: 1456 09/11/97
.. 79
-------
Page No. 6 Listing of S975808B.dbf
09/11/97 Matched GC Peaks / Ratio / Ret. Time
Compound/
H_2 QC.Log Omit Why ..RT. OK Ratio Total. Area... Area. Peak. 1.. Area. Peak. 3.. Rel.RT Compound.Name.. ID.. Flage.
OCDD 0.76-1.02 0.884-1.116
458-460 DC ML 0:00 0.86 0.13 0.000
34:33 0.87 13,207.19 5,681.55 6,525.64 1.000 OCDD AN
458-460 1 Peak 12,207.19
13C12-OCDD 0.76-1.02 0.996-1.005
470-472 DC NL 0:00 RO 1.17 0.11 0.000
34:32 0.86 1,984.37 920.29 1,064.08 1.000 13C12-OCDD ZS8
DC WH 34:55 0.76 2.02 1.011
470-472 1 Peak 1,984.37
Col nan Description 'Why* Code Description QC Log Desc.
M_Z -Nominal Ion Mass(es) WL-Below Retention Time Window A-Peak Added
..RT. -Retention Time (CUB:SB) WH-Above Retention Time Window K-Peak Kept
Rat.l -Ratio of M/M+2 Ions SN-Below Signal to Noise Level D-Peak Deleted
OK -RO-Ratio Outside Limits
-------
rilatS975808 tl-848 Aoq:10-SEP-1997 21:08:49
EI+ Voltag* SIS 70S Hoimmi28
303.9016 r:2 BSUB(256,30e-3.0) PXD(9,5,5,0.05\,112.0,1.00\rr,T) ExptXPCOS
TRIANGLE LABS TfXtiI-M23-l TLIt43057
1001
sol
60:
•
401 A1.10X5 JU.04
20: A4.46E4 A 11 \h Jl
o\J\ J^ jVjpi/ *i(*r \A. / VN_/ \
17:00 18:00 ' 19:00
.£110:5975808 tl-848 AcgslO-SEP-1997 21:08:49
INJ. TIME - 21:11
A3. 23X5 -6.1X4
I
A1.67E5 \\
A6.43E4JI 1]
ZS 1 J 1 AS 07E4 A6.59X4
Jl fl 1 1 *A5T 1 '[A4.72X4 k
^r*H\/ L-Ai^i v»^ ^\^n\,^J^*^l/\^ ..„ /\ .f A. A
^4.9S4
LJ.7E4
L2.5B*
Ll.2Z4
- o.oro
20:00 ' 21:00 ' ' 22:00 I*J»e
El* Voltag* 5ZX 705 Jtol*«i20ff
305.8987 T:2 BSOB(256t30,-3.0) PB>(9,S,5,0.05\,824.0,1.00\,r,T) ElptEPCUS
TRIANGLE LABS Text J-T-.M2.3-i TLH430S7
1003
80:
601
401 ,, ,,
; A1.36E5 S
20^ il J( A /I
«: _AU *?J£Ej\^ .AvXY /MjLJl
17:00 18:00 19:00
ril«:S97580S #1-848 Acg:10-S£J>-1997 21:08:49
XNJ-. TIME - 21:11
A4.32ES
I
X5 * A 1
Jl A8.54JT4
A/kA / A / i ^-tlr< A1.90S4 A6'^X4
rJ^\f V/ LVV/ V_^ /IWV.. _v .^IA^JIVI ^r\..lMJJ^
_ff.5W
.6.8X4
.5-1X4
'.3.4X4
Li. 714
-O.OEO
20:00 21:00 22:00 ' HM
ri-f Voltag* 5IX 705 Mbia«;440
315.9419 Ft2 BSOB(256,30,-3.0) PKD(9,5,5, 0.05\,1760.0,l.OO*,r,T) ElptEPCUS
TRIANGLE LABS Te3Ct:I-M23-l TLH430S7
1001
80:
60:
40:
20:
a-
17:00 18: 00 19:00
INT. 3ZME - 21:11
A2.60E7
|
| \
_ff.2Eff
L5.0rff
j.3.7*ff
.2.5X6
'-.1.2X6
•o.oxo
2olfl<7 21:00 22ioO Tdmm
T±ietS975808 tl-848 AcqtlO-SEP-1997 21:08:49 EI+ Voltage SIX 70S Naif at 587
317.9389 T:2 BSUB(256,30,-3.0) PKI>(9,5,5,0.05\r2348.0r1.00\,T,T) ExptEPCOS
TRIANGLE LABS Text : J-K23 -1 TLIt43057
1001
80:
60:
40:
20:
"' 1
17:00 10:00 19:00
HKT. TIME - 21:11
A3. 43X7 -8.1X6
ft
\
.6.5X6
.4.9X6
.3.2X6
.1.6X6
0.0X0
20 i 00 21:00 22:00 Time
Til»iS97580a tl-848 AcqslO-SEP-1997 21:08:49 EH- Voltage SIX 705
330.9792 T:2 ElptEPCUS
TRIANGLE LABS Tert:I-M23-l TLI943057
1001
°°- .... 17,35 ^^^A^--^
60:^^^^^^ ^^
40:
20:
ol
17:00 18:00 19:00
JWJ. TTME - 21:11
21:45 22»21 ^5.4X6
15:48_*°y* 20 : 54^>,>^««vyys^Sv*-^^^^V>y^N*O'v
.4.3X6
.3.2X6
.2.1X6
-.1.1X6
•o.oxo
20:00 21:00 22:00 Xiaia
ril»:S975808 tl-848 AcqtlO-SEP-1997 21:08:49 EI+ Voltag* SIR 70S
375.8364 F:2 XxptEPCUS
TRIANGLE LASS T*xttI-M23-l TLH43057
1001
80:
60:
XK7. TTM7 • 21:11
21:2J 2I 5S pl.lW
19:45
: 17:10 19»10 ,,. ,«
*0m. . 17:42
301 1 1 11 «*lel37 IS I
o '• LftAjlMLhuJWA/U!^^
17:00 18:00 19:00
«« I J^
20. JO , I
LviuJuUuLjJlLAj^
.9.0X3
.6.8X3
.4.5X3
.2.3X3
'• 0 . OfO
20:00 21:00 22:00 Ti»«
81
-------
'lle,S975S08 H-848 AcqilO-SEP-1997 21i08i49 XH- Voltage SIS 70S Boife,34
319.8965 F,2 BSUB(256,30, -3.0) PKD(7, 5,3,0 .OS\,136 .0,1.00\,F,T) XxpiXPCUS
TRIANGLE LABS Text:I-H23-l TLH43057 HKT. TXMX - 21(11
1001
19(00 20(00 21(00 22(00
rlletS975808 H-848 Acq<10-SEP-1997 21(08(49 EI+ Voltage SIS 70S SO±M»t2Sa
321.8936 F:2 BSUB(256,30,-3.0) PKD(7, 5,3,0.05\,1036.0,1.00\,F,T) XxpiXPCUS
TRIANGLE LABS TextiI-M23-l TLH43057 1K7. TXMX - 21 til
1001
f .,i.i*.> |TnT|.i fTf,-r—it ~fi r, i-y
19,00 20t00 21i00 22(00
F11*:S975808 H-848 AcgtlO-SXP-1997 21:08:49 XH- Voltage SIS 70S Noime:617
331.9368 Fs2 BSOX(256,30,-3.0) PXD(7,5,3,0.05\,2468.0,1.00\,F,T) ElpiEPCUS
TXIAKGLE LABS Text,I-M23-l TLH43057 ntr. TIME - 21:11
1001
so:
60.
40.
20:
o:
I
~^$p
19(00 20(00 21(00 22(00
File,3975808 H-848 AcqtlO-SEP-1997 21(08(49 EH- Voltage SIS 70S Hoiae,35
333.9338 F:2 BSOB(2S6,30, -3.0) PXD(7,5,3,0.05\,140.0,1.00\,r,T) XxpiXPCUS
TRIANGLE LABS Text:I-K23-l TLH43057 UKT. TIME <• 21(11
1001 A2.47E7
sol
601
401
201
20(00 21(00 22(00
Fil»iS975808 H-848 Acq,10-SEP-l$97 21:08,49 EI+ Voltage SIS 70S Ko±fe:502
327.8847 F,2 BSOB(256,30, -3.0) PXD(7,5,3,0.05\,2008.0,1.00\,F,T) XxpiXPCUS
TRIANGLE LABS Text:I-M23-l TLH43057 ZK7. TIME - 21:11
1001 A1.B1EB
801
601
401
30j ', ', -3.63X7
A
20(00 21(00
r±leiS975808 fl-848 AcqilO-SEP-1997 21:08:49 ZH- Voltage SIS 70S
330.9792 Ft2 ExptXPCUS
TRIANGLE LABS Text:I-H23-l TLH430S7 1X7. TIME
1001
19.48 ™L"_ 20(54
80J
60:
401
201
0.
22(00
T±m
.2.1X6
.1. 0X6
.0.0X0
Tim,
.6.5X6
.5.2X6
.3.9X6
.2.6X6
.1.3X6
.0.0X0
Tim^
4.1X7
3.3X7
2.4X7
1. 6X7
a. 1x6
o.oxo
Tim
-5.4E6
.4.3X6
.3.2X6
.2.1X6
.1.1X6
19(00
20(00
21(00
22(00
0.0X0
Tim
82
-------
rila:S975808 rl-848 AcqtlO-SXP-1997 21:08:49 Eli- Voltage SIX 70S Noil* 1 35
339.8597 Ts2 BSUB(256, 30, -3.0) PXD(7,5,3,0.05\,140.0f1.00\,r,T) ExpiXPCOS
TRIANGLE LABS T*rt>I-M23-l TLH43057
1003
sol
tfoj
40:
20:
o-
A2.47E5 A3. 21X5
ft
\ 1
L.70E
T A
/ \ A1.01E4 A l\
A 1 W A- _rU r\_/
23iOO ' 24 tOO
OKT. TIME - 21 ill
Al . 78E5
i
A1.00C5 ft
A1.58r5 ll M A7.34W
t\J\ ffn n Mil n A2 15E4
A. / 1 / V\ f\ 1 1 t I \ / \ A3..66E4 )\ k ~L i
I U / V -^ ^ *-r ^i T-'V1— V -* LJ^^^ ji--"/l
.7.3X4
-.5.8X4
-.4.4X4
'-2.9X4
•_1.5X4
0.0X0
25 100 26:00 Tim*
file :SS 758 08 tl-848 AcqtlO-SXP-1997 21:08:49 EH- Voltage SIX 70S HOiM*i46
341.8567 Fi2 BSUB(256, 30, -3.0) PXD(7, 5,3,0. 05\,184. 0,1. 00\,r,T) XrptXPCOS
TRIANGLE LABS T*Xt:I-M23-l TLH43057
1001
80:
60:
40:
20:
0:
{'5
-
A
Av.
' 23\00 24iOO
UKT. TIME • 21 ill
A1.21X5
Jl A6.64E4
A1.07X5 A4.79E4 n\A9.02X4 A
' 1 Jl A. /I 1 l\ &1'25E4 \ AiM M .« 77 r<
J| 1"^ -"M Afl 1 Illl '^ 901M Ml i"l k
/ »wv/V M J If »^A/Yy \ r*Jl- /" W V^A ~/1VA >> JV VA/^VAA/^ V A/I
-5.3X4
14.2X4
.3.2X4
.2.1X4
.1.1X4
.0.0X0
25 loo isloo n««
rile:S975808 tl-848 AcqslO-SXP-1997 21:08:49 EH- Voltage SIX 70S Boil*: 42
351.9000 1:2 BSOB(256,30,-3.0) PXD(7,5,
TSIANGLE LABS T*XtiI-M23-l TLH43057
1001
80:
60:
40:
20:
0:
23\00 24:00
j,o.05%,i«8.o,JL.oo%,jr,r; xxptxpcos
nor. TIME - 21 ill
Aa-?5*7 A2.69E7 C*'5*'
(1
/ V /I
'.7.6X6
-.3.7X6
'•.3.8X6
'-1 .9X6
'• o . oxo
25 100 2«iOO Ii««
rile:S975808 tl-848 AcqtlO-SXP-1997 21:08:49 Eli- Voltage SIB 705 Hoi**t3S
35J.8570 F:2 BSUB(256,30,-3.0) PXD(7,5,
TSIANGLE LABS T*xtsI-M23-l TLIt43057
1001
80:
60:
40:
20:
0:
23iOO ' 24iOO
•3,o.o5%,i40.o,i.oo%,r/r; xrpixpcas
IJU. TIMS - 21)11
A2.08I7 A1.86E7
n
/ V /I
-6.6X6
l5. 3X6
14 . 0X6
'-.2.6X6
.1.3X6
0.0X0
25:00 26 1 00 Tim*
rileiS97580a tl-848 AcqtlO-SXP-1997 21:08:49 EH- Voltage SIB 705
330.9792 T:2 ExpiEPCOS
TXIANGLE LABS Text:I-H23-l TLIt43057
1001
80:
60:
40:
20:
o:
^^>v-VW^A^^AXv-^vV/V^V^r^^nJ**W'
UKT. TIME - JJljll
24:2ff24«42 25.-06 35»37 26:03 2ffA£L^26:47 r-ff-<**
vw— ^X\^W — <^vv\j-v^V\ f*^^~~*r'~v~~J^\r~iAf^*~^~*' •*C-~ v^^.
'•.5.1X6
.3.3X6
.2.6X6
.1.3E6
'• o . oxo
23tOO 24\00 ' ' ' 25'tOO 26>00 Tim*
rile:S975BOa tl-848 AcqtlO-SXP-1997 21:08:49 EI+ Voltage SIX 705
409.7974 T:2 ExptXPCOS
TSIANGLE LABS T*xtiI-K23-l TLH43057
1001
80:
60:
40:
201
o:
23{°6 33'35 \3'43
uMA^^/L-^sAAA-J^-AAM-JOv,,^ V
ZIK7. TX«T - 21/11
^1.5X4
}»JMIW£LJL]^^
'.1.2X4
.9.2X3
.6.2X3
.3.1X3
• o.oro
2jloo 24 100 25 100 2«loO X±m*
83
-------
FileiS97580a H-B48 AcqilO-SEP-1997 21lOBt49 EI+ WUtagv SZX 70S
MKl**lJ4
355.8546 r>2 BSUB(356,30,-3.0) PKD(7,5, 3, 0.05%,1 36. 0,1. 00\,T,T) XxptXrCUS
TSIAHSLX LABS T«zt:I-K3J-l TLIt43057 IKT.
1001
SO.
60.
40.
20.
01
A3.36E5
A
rt
\ «.I«5 U.ua U.73H *'•!"*
\ I K A A1.07E5 A\
1 r 1 \\ 11 l\ A A I ' U
ma - 21 til
III II Mil /lr\/ 1 1 '* ** *.,,/,«,. A3. 52X4
J \)\^J 1/v V wif V/An./XjA ^ A Aa-xfl5L
24iOO 25'iOO
rilasS975808 H-848 AcqtlO-SXP-1997 21:08:49 XH- Voltfgv SIX 70S
.7.0X4
.5.6X4
.4.2X4
.2.8X4
.1.4X4
0.0X0
26 1 00 UM»
HOlf»i39
357.8516 Ft2 BSUB(256,30, -3.0) PXD(7,5, 3, 0.05%, 156. 0,1. 00\,T,T) XxpiXPCUS
TRIANGLE LABS TextiI-M23-l TLIf43057 1X7.
1001
80.
60.
40.
20.
0.
A4 01X7
A8.46E6
II A
24sOO 25iOO
rll«,S975808 tl-848 AoqilO-SEP-1997 21i08t49 XI+ Voltaga SIX 70S
Tna " 21:11
-1.3X7
.1.0X7
.7.6X6
.5.1X6
.2.5X6
0.0X0
26\00 ' • • • • ziaa
H0if»t35
367.8949 Ti2 BSOB(256, 30, -3.0) PKD(7, 5,3,0. OS\,140 .0,1. 00\,T,T) XxpiXPCUS
TXIASSLX LABS Tttxt.1 1-M23-1 TLH43057 OKT.
ion
80.
601
40.
20.
0
Al
/
24:00 ' 25 i 00
riletS975808 91-848 AcqtlO-SKP-1997 21:08:49 XI+ Voltaga SIX 70S
ma - 21 ill
11X7
1
Wi.77rff
vvv
-.5.9X6
.4.7X6
.3.5X6
.2.3X6
.1.2X6
0.0X0
26*00 Tiaa
naif u t 33
369.8919 T:2 BSUB(256,30,-3.0) PKD(7, 5,3,0. 05\,132. 0,1. 00\,r,T) XxpiXPCUS
TRIANGLE LABS Text.-J-MZJ-l TLH43057 HOT.
1001
801
601
401
201
0'
Al.
J
24\00 2S\00
rll»iS975B08 #1-848 Aci
6.4X6
.5.1X6
.3.9X6
.2.6X6
.1.3X6
0.0X0
26\00 ' ' Timm
84
-------
rll»:S975808
373.8208 Fi3
TRIANGLE LABS
100]
80:
50:
40:
20:
A3.
A1.32.E5
J
27:24
r±20:S975S08
375.8178 rs3
#1-405 AcqtlO-SEP-1997 21:08:45 EI+ Voltag* SIS 70S Hoiami563
BSVB (256,30, -3.0) PKD(7,5,3,0.05\t22S2.0r1.00\fTtT) XxpiXPCOS
T«xt:I-H23-l TLIH3057
61X5
A
\
\
U
A4..
Al . 7S£5 I
A 1
AS . 0424 \ /
• ««A / I /
3*5
ft
IXT. TIMX - 21:11
A2.15r5
\ / \ A5.43*4 J\
V vyv^v^x 7 V _j,
27:35 27:48 28:00 28.12 28:24 28:35
28:48' 25: 00 ' 25:12' 25:24
A8.55JE4
trr^/YVrrr^f{Lf Ty»«VA
J..2XS
.5.8*4
.7.3*4
.4.9*4
.2.4*4
Lo . ozo
25:36 25:48 30:00 30:12 Time
#1-405 AcqsLO-SEP-1997 21:08:45 EI+ Voltagr* SIS 70S Noif»:434
£502(256,30, -3.0) PXD(7,5,3,O.OS\,1736.0,1.00\rT,T) ErpiEPCUS
TRIANGLE LABS
1001
so:
60:
40:
20:
A2
A8.69X4
A)
27:24
F±1»:S975808
383.8639 F>3
Tazt:J-M23-l TLH43057
64X5
A
1
I
A3. 1715
A
AI-AJ8r5 n1-?**5
\ A
l\ 1 11
^A /L J VU"
27:35 27:48 28:00 28:12 28:24 28:35
IXT. TIMX - 21:11
A1.35S5
28:48 '25: 00 ' 25:12' 25:24'
AS. 83X4
-9.0*4
:7.2*4
15.4*4
13.6*4
11.8*4
-0.0*0
25:36 25:48 30:00 30:12 TlJia
#1-405 Acq:10-SEP-1997 21:08:45 EI+ Voltigm SIS 70S No±**:1126
BSUB(256,30,-3.0) PXD(7,5,3,0.05%,4504.0,1.00%, J,T; Elp:EFCUS
TRIANGLE LABS
100}
80:
60:
40:
20:
o:
27:24
F±le:S97580a
385.8610 F:3
2
Text.r-K2.3-l TU #43057
Al 39X7
j
V V
6 27:48 28:00 28:12 28:24 28:35
OKT. TIMX - 21:11
!<••»
;
±- y* /\^^>^V _A iw\ ^-ftjYji_fVV/V*/J'jr~t^''^M\J>/^^AA^ ^^^vyv/^^^
•~'~>v\s/vrvv/vA/~v^^' *>r *~ v
27:36 27:48 28:00 28:12 28:24 28:36
!*• >^ - \ J*" VV^y »^'- --
28:48' 25:00 25:12 25:24
-2.5**
.2.3X6
.1.7X6
.1.2X6
.5.8X5
0.0X0
25:36 25:48 30:00 30:12 H»«
#1-405 Ac?:10-S£P-1557 21:08:45 EI+ Voltage SIS 70S
XxptXPCOS
TRIANGLE LABS
100]
80:
60:
40:
20:
o:
T«xt:X-K23-l IXJ #43057
27:33
JLJLJ
27:24
L
28:10
JLJLuVN^AjlJ^
27:36 27:48 28:00 28:12 28:24 28:36
XNT. riMT - 21:11
-1.0X4
25:30
•4T° "*"T5
AJUUMAA/^/vUJLAAMA.
28:48 29:00 29:12 29:24
25:59 1
1 29t]f4\ 1 1 jll 1 1 I
.8.3X3
.6.2X3
.4.2X3
E.2.1IJ
r 0.0*0
29:36 29:48 30:00 30:12 TLm»
85
-------
Leisy/seua tJ.-4U3 AcqtJ.0-SEP-J.yy/ iitoatts sir- voitmg* SIX 70S Rolf*:733
389.8156 rs3 BSUB(256,30,-3.0) P1O}(7, 5,3,0.051,2892.0,1.00\,r,T) XxptEPCOS
TRIANGLE LABS T»It:I-M23-l TLH430S7 IXT. TIME - 21ill
1004 AS. 59X5
27:46 28:00 28:12 2Si24 28:36 28>48 29:00 29il2 29i34 29i36 29', 48
F±l«sS975808 tl-405 Acq, 10-SEP-19 97 21:08,49 XI+ Voltaff* SIX 70S Noll*,467
391.8127 Ft3 BSVB(2S6,30,-3.0) PJO3(7,5,3, 0.05\,1868.0,1.00\,r,T) XxptXPCVS
TRIANGLE LABS TmxtiI-M23-l XLH43057 HOT. TU4X - 21:11
1003, A4.72X5
27,48 28,00 28', 12 28*24 28', 36 28:48 29:00 29', 12 29t24 29:36 29,48
r±l»tS975808 il-405 AcqtlO-SEP-1997 21,08,49 XI+ Voltage SIS 70S ttoiem,401
401.8558 F:3 BSUB(256,30,-3.0) PKD(7,5,3,0,05\,1604.0,1.00\,r,T) EiptEPCUS
TRIANGLE LABS Text,I-H23-l TLH43057 ZK7. TIMS - 21 til
ao:
60.
40.
20.
0.
A4.16E5
A3.84S5
Al. 61E5
A9.67E4
A -
12E4
A2.23K5
so:
ffOJ
40:
20:
A3.42ES
A2.97ES
A1.39E5
A8.20E4
A2.04E5
A3.38S4
1001
so:
so:
40:
20:
A1.63E7
Al. 74E7
27:48 28,00 28:12 28:24 28,36 28,48 29:00 29,12 29,24
r±letS97580a il-405 AcqtlO-SEP-1997 21:08,49 EH- Voltag* SIS 70S Noif*:484
403.8529 r,3 BSUB(256,30,-3.0) PXD(7,5,3,0.05\,1936.0,1.00\,r,T) ExptEPCUS
TRIANGLE LABS Teit:I-M23-l TLH43057 IJU. TIME -
29:36
29:48
10 03
80.
50.
40.
20.
0.
A1.42X7
A1.32E7
27*48 28:00 28,12 28:24 28:36 28:48 29:00 29:12
rilt>S97580a #1-405 Acq,10-SEP-1997 21:08,49 11+ Voltay* SIS 70S
392.9760 Ti3 XxptXtCOS
29,24 29:36 29:48
TRIANGLE LABS Tfxt:I-N23-l TLH43057
1003
ao:
60.
40.
20:
0.
23:30
28,46
INJ-. TIME - 21:11
.1.7X3
.1.4X5
.1.OXS
.7.0X4
.3.5X4
0.0X0
Tim*
1.5X5
1.2X5
9.0X4
6.0X4
.3.0X4
.0.0X0
Time
.6.8X6
.5.5X6
.4.1X6
.2.7X6
.1.4X6
0.0X0
Time
^X^JW^W*^^
27,48 28,00 28,12 28:24 28,36 28,48 29,00 29:12 29,24 29:36 29,48
.5.8X6
.4.6X6
.3.5X6
.2.3X6
.1.2X6
.0.0X0
Time\
.2.9X6
.2.3X6
.1. 7X6
.1.2X6
.5.8X5
.0.0X0
Time
86
-------
T±1»:S975B08 tl-430 AcqtlO-SEP-1997 21*08*49 EI+ Voltage SIX 70S No±M»:1412
07.7818 r:4 3503(256,30,-3.0) PJO)(7,5,3,0.05\,564a.O,1.00\,T,T) XxptEPCOS
TBIAXGLE LABS Text:I-M23-l 1X1*43057 XK7. TIME - 21 ill
1001 A6.9.5E5
T
T
' ill 12 3l't24 31*36 31*48 32:00 32:12 32t24
fileiSS75808 tl-430 AcqtlO-SEP-1997 21t08t49 EI+ Voltage SIX 70S Xoim»>862
409.7789 rt4 3SUB(256,30,-3.0) PXD(7,5,3, 0.05%,3448.0,1.00%,T,T) XxptSPCOS
TRIANGLE LABS T*Xt:I-M23-l 1X1*43057 IKT. TIKE - 21 til
60:
40:
20-.
A3.98E5
A8.73E4
A
Al.05X5
A2.26X4
ft-
32t36
32:48
1003
80:
so:
40:
20:
A4.54E5
A3.88E5
A7.91E4
y^
Ai.oess
' ' ' 31t36
' ' ^ 31\1231lt24' ' ' 3l'*36' ' 31,48 32iOO 32il2 32i24 32:308i49 EH- Vtoltag* SIX 70S Jfc>i««i7JO
rs4 3SVB(256,30,-3.0) PKD(7,5,3,0.05\,2920.0,1.00\,T,T) XipiXPCUS
TBIANGLE LABS T*xttI-M23-l TLIt43057 UKT. TIME - 21 til
1001 Al 3SE7
32:48
80:
60:
40:
20:
A9.10E6
31.12 31:24 31:36 31:48 32:00 32:12 32:24 32:36 32:48
rile:S97S808 tl-430 AcqilO-SEP-1997 21*08:49 EH- Voltage SXX 70S
430.9725 T:4 Exp-.EPCUS
TRIANGLE LABS Tejrt:I-M23-1 TLH43057 UKT. TIKE - 21:11
32:04 32:22 32:3332:40
.1.8X5
Ll.425
.1.1X5
.7.1X4
.3.5X4
.0.0X0
.2
a.
.1.
.8.
.4.
0.
6X5
3X5
5X4
3X4
2X4
0X0
Td**\
2X6
8X6
3X6
9X5
5X5
0X0
ao:
60:
40:
20:
32:50
31:07
31:15
31:28
31:12 31:24 31:36 31t48 32:00 32:12
r±la:S975808 tl-430 AcqilO-SEP-1997 21*08*49 EH- Voltage SIX 70S
479.7165 T:4 Ezp:EPCUS
TRIANGLE LABS Text:I-M23-l TLH430S7 ItU. TIMS
lOOi
80:
so:
40:
20:
o:
32*24
32:36
32:48
32:24
32*50
31*12
31124
31136
31:48
32:00
32:12
32*24
32:36
0X6
0X6
0X6
0X6
,0X6
.0X0
HMO
.4X6
.9X6
,4X6
.5X5
.7X5
.0X0
T±M*H
.7X3
.7X3
.BX3
.9X3
.4X2
.0X0
ri««|
87
-------
lJ.asS975BUa H-43O AcqiJ.0-SEr-S.9S7 21tQ8t4yEI+ Volt&ya SIX 70S Half»:1429
423.7766 Ti* BSUB(256,30,-3.0) PKD(7,5,3, 0.05\,5716.0,1.00\,r,T) ExptEPCUS
TRIANGLE LABS T*xt:I-M23-l TLH43057 INJ. TIKE - 21 til
1001 A3.27X6
31:18 31:24 31:30 31:36 31:42 31t48 31,54 32:00 32:06 32:12 32tl8
F±le:S975808 41-430 AcqilO-SXP-1997 21i08i49 EI+ Voltmgm SIS 70S Koimmt822
425.7737 T:4 BSUB(2S6,30,-3.0) PXD(7,5,3,0.05\,3288.0,1.00\,r,T) Exp:EPCOS
TRIANGLE LABS Tait:I-M23-l TLH430S7 IBJ. TXMT -
1001 A2.37E6
80.
60.
40.
20.
A1.91E6
.8.6X5
".6.8X5
15.1E5
.3.4X5
.1.7X5
32:24 32:30
0.0X0
T±m>
80.
60.
40.
20.
A1.95E6
31:13 31324 31:30 31:36 31:42 31:48 31:54 32tOO 32:06 32tl2 32:18
rlle:S975808 41-430 AcqtlO-SEP-1997 21:08:49 EI+ Voltaye SIX 70S Nt>±ia:826
435.8169 T:4 BSUB(256,30,-3.0) PKD(7,5,3,O.OS\,3304.0,1.00\rr,T> ExptEPCUS
TRIANGLE LABS TfXttI-M23-l TLIt43057 1X7. TIME - 21sll
1001 A1.Q2E7
80.
60.
40.
20.
.8.0X5
-7.0S5
_5.3r5
_3.5«5
.1.0X5
0.0X0
32:24 32:30
,.3.6X6
.2.9X6
.2.2X6
'.1.4X6
.7.2X5
31:18 31:24 31:30 31:36 31:42 31:48 31:54 32:00 32:06 32:12 32:18 32:24
riletS975808 #1-430 AcqtlO-SEP-1997 21:08:49 XI+ Voltagm SIS 70S Nol*»,676
437.8140 T:4 BSUB(256,30, -3.0) PXD(7,5,3,0.05\,2704.0,1.00\,f,T) ExptEPCUS
TXIANGLS LABS Text»I-H23-1 TLH43057 UKT. TIME - 21:11
1001 A9.93E6
so:
40.
20:
32:30
0.0X0
TiM
.3.4E6
'.2.7X6
.2.0X6
.1.4X6
.6.8X5
31:18 31:24 31:30 31:36 31:42 31:48 31:54 32:00 32:06 32:12 32:18 32:24
F±le:S975808 #1-430 AcqilO-SEP-1997 21:08:49 EI+ Voltag* SIR 70S
430.9729 Tit XxptXPCaS
TRIANGLE LABS Tmxt,I-M23-l TLH43057 IKT. TIME - 21 ill
32:30
0.0X0
Tim*
100]
80.
so:
40:
20:
31:20
31:39 31:46
31:54
32:04
,.2.3X6
.1.9X6
.1.4X6
.9.4X5
.4.7X5
31:18 31:24 31:30 31:36 31:42 31:48 31:54 32:00 32:06 32:12 32:18 32:24 32:30
0.0X0
Tim
-------
File:S975SOa tl-430 Acq:10~SEP-1997 21:08:49 EI+ Voltmf* SIX 70S Bait*:32
441.7428 Tit BSOB(256r30,-3.0) PXD(7,5,3,O.OS\,13».Or1.00\,T,T) ExptEPCUS
TRIANGLE LABS Tert:I-K23-l TLH43057 JJW. TXMX - 21 ill
1001 A3.86X5
901
8 01
601
50J
40.
20.
101
A9.53E3
„ A .
A1.86E4
A4.73E3
A9.55E3
31:00 32:00 33:00 34:00 35:00
rlletS975808 tl-430 Aog:10-SEP-1997 21:08:49 EI+ Voltage SIS 70S Oolu*i33
443.7399 Tit BSUB(256,30,-3.0) PXD(7,5,3,0.05\, 132.0,1.00\,T,T) ExptEPCUS
TSIANGLE LABS Taxt:I-H23-l TLH43057 UKT. TIME - 21*11
1001 A3.78E5
901
801
701
601
501
401
201
lol
OJ
A3.81E3
A8.62X3
^/\_ JH. ^WL
31:00 32:00 33:00 34:00 35:00
rlletS975808 tl-430 AcqtlO-SEP-1997 21:08:49 EI+ Volttgm SIX 70S
430.9729 T:t ExptEPCUS
TRIANGLE LASS Text:I-H23-l TLIt43057 IKT. TIME - 21:11
30s5s *,.**,*.** 32s.so 33:34 33:57 34>33 34:55
31:00 32:00 33:00 34:00
ril0:S97S808 tl-430 Accj: 10-SEP-19S7 21:08:49 EI+ Voltay* SIS 70S
513.6775 F:4 ExptEPCdS
TRIANGLE LABS Text:I-M23-l TLH43057 IKT. TIME - 21 ill
100!
90.
80.
701
60. 34:38
501
40.
20.
101
35:00
35
31 tOO
30:45
32:55 341 11
.Ji-JkMjLLjt^^
13
35:34
J4-.50
7E4
9E4
1X4
4E4
6E4
8E4
1X4
3X4
5X4
7X3
0X0
6X4
8X4
1X4
3X4
6X4
8X4
0X4
3X4
5X4
6X3
.0X0
T±m*\
ulLJ
31iOO
1X3
2X3
2X3
3X3
4X3
5X3
6X3
7X3
8X3
1X3
0X0
32:00
33:00
34100
35:00
89
-------
y/yauti rj.-iju Acqij.u-SEf-j.yy/ jj.,uvtiy an- voj.uaym SIM /us
457.7377 Ti4 BSOB(256,30, -3.0) PO>(7,5,3,0.05%, 120.0,1.00\,r,T) ExpiEPCOS
TXIANGLE IABS Tmxt,I-M23-l TIJ943057 IKT. TIMS - 21 ill
1001 A5_J8E7
34:24 34:30 34i36 34t42 34:18
Fll»:S975808 H-430 Acq, 10 -SEP -19 97 21t08:49 XH- Voltage SIX 70S Hoit»t33
459.7348 Ft4 BSUB(256, 30, -3.0) PXJ>(7,5,3,0.05\,132.0,1.00\,r,T) ExptEPCOS
TXIASSLX LASS Text,I-H23-l TLH43057 IKT. TIMS -
1001 A6J3X7
34,24 34:30 34,36 34,42 34,48 34,54
Tile,3975808 #1-430 AcqtlO-SEP-1997 21:08:49 EH- Voltaga SIS 70S Hoi**133
469.7779 F:4 BSUB(256,30,-3.0) PXD(7,5,3,0.05\,132.0t1.00\,r,X) ExptXPCUS
TSIAHSLE LABS Text,I-H23-l TLH43057 OKT. TIME - 21:11
1001 A9.20E6
34,54
34:24 34:30 34,36 34,42 34:48
rll»,S975808 tl-430 Acq:10-SEP-1997 21,08:49 EH- Voltaya SIX 70S Noil*,30
471.7750 r,4 BSUB(256,30,-3.0) PJO>(7,5,3,0.05\, 120.0,1.00\,r,T) ExptEPCUS
TXIA1KLX LABS Text,I-M23-1 TLH43057 IKT. TIME -
1001 A1.Q6E7
34:54
34,24 34,30 34,36 34,42
r±l»:S975808 tl-430 AcqtlO-SEP-1997 21,08,49 EH-
430.9729 r,4 ExpiEPCUS
TRIANGLE LABS T*Xt:I-H23-l TLH43057
100J
00J
60.
40.
20.
0.
34 > 26
34:33
34:48
SIX 70S
IJW. TIME -
34,49
34:54
21,11
34,55
-1.4E7
.1.1X7
.8.3X6
.5.5X6
.2.7X6
.0.0X0
35:00 Tim*
-1.6X7
-1.3X7
.9.5S6
.6.3X6
.3.2X6
.0.0X0
35', 00 Tim>
.2.3X6
'-1.8X6
-1.4E6
.9.1X5
.4. 6X5
0.0X0
35:00
Tim*
. 7X6
12.1X6
'.1. 6S6
.1.1X6
.5.4X5
.0.0X0
35:00 TimeA
.2.4X6
'.1.9X6
.1.4X6
.9.5X5
.4.8X5
34,34
34:30
34,36
34t43
34:48
34154
.0.0X0
35100 T±mm
90
-------
T6
-------
92
-------
CO
File;597580fl #1-848 Acq;10-SBP-1997 21;OB;49 B1+ Voltage SIR 705
319.8965 F:2 Exp:EPCUS
Sample Text:I-M23-l TLI#43057 INJ. TIME -
lOOt
21:11 File Text:I-M23-l TLII4»
r_1.3E4
20:00 21:00
File:S975808 #1-848 Acq:10-SEP-1997 21:08:49 EI+ Voltage SIR 70S
321.8936 F:2 Exp:EPCUS
Sample Text:I-M23-l TLUU3057 INJ. TIME -
10 OS.
22:00
.O.OEO
Time
21:11 File Text:I-M23-l TLI#4»
..4.4E4
20100 21:00
File:S975808 ttl-848 Acq:10-SEP-1997 21:08:49 EI+ Voltage SIR 70S
331.9368 F:2 ExprEPCUS
Sample Text:I-M23-1 TLI#43057 INJ. TIME =
lOOi 21;01 21:13
80J
60 j
40J
20 j
22:00
O.OEO
Time
20:00
21:11 File Text:I-M23-l TLI#4»
r5.2E6
_4.2E6
_3.1E6
_2.1E6
-1.0E6
21:00
22:00
_O.OEO
Time
-------
Flle:S975808
339.8597 F:2
Sample Text:
1004
80 j
60 j
40J
20J
/
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23:36
File:S975808
341.8567 F:2
Sample Text:
1004
80 j
60 j
40 j
20 j
0-
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23:36
File:S975808
351.9000 F:2
Sample Text:
1004
80.
60J
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-------
TLI Project 43057
Client Sample: I-M23-1
Method 23 TCDD/TCDF Analysis (DB-225)
Analysis File: X973082
Client Project
Sample Matrix:
TLI ID:
Sample Size:
Dry Weight
GC Column:
M23TRAIN
181-27-1A-C
1.000
n/a
DB-225
Date Received: 08/29/97
Date Extracted: 09/06/97
Date Analyzed: 09/11/97
Dilution Factor: n/a
Blank File: S975807
Analyst MS
Spike File:
ICal:
ConCat
% Moisture:
% Lipid:
% Solids:
SPC2NF04
XF24087
X973069
n/a
n/a
n/a
EMPC
0.02
B_
»C,r-2,3,7,8-TCDF
2.9
73.7
40%-130%
0.79
22:31
"CB-1A3.4-TCDD
0.76
21:30
Data Reviewer.
Page 1 of 1
09/12/97
UO. LAKS & KUM
Triangle Laboratories, Inc.*
801 Capitola Drive • Durham, North Carolina 27713
Phone: (919) 544-5729 • Fax: (919) 544-5491
Printed: 14:58 09/12/97
-. 100
-------
Initial
Data Review By:
Calculated Noise Area: n/a
The Total Area for each peak with an ion abundance ratio outside
ratio limits has been recalculated according to method requirements.
Page Ho.
09/12/97
Listing of X973082B.dbf
Hatched GC Peaks / Ratio
/ Ret. Tiae
Compound/
M_Z QC.Log Omit Why ..RT. OK Ratio Total.Area... Area.Peak.1.. Area.Peak.2.. Rel.RT Compound.Name.. ID.. Flag*.
TCDF
304-306
MK
304-306
13C12-TCDF
316-318
DC
DC
DC
DC
DC
DC
DC
DC
DC
DC
DC
DC
DC
DC
DC
DC
DC
DC
DC
DC
DC
DC
DC
DC
DC
DC
DC
DC
DC
DC
DC
DC
DC
DC
DC
DC
DC
DC
NL
SN
SN
SN
SN
SN
SN
SN
SN
SN
SN
SN
SN
SN
SN
SN
SN
SN
SN
SN
SN
SN
SN
SN
SN
SN
SN
SN
WH
1
NL
WL
WL
WL
WL
WL
WL
SN
SN
0:
18:
18:
18:
18:
18:
19:
19:
19:
20:
20:
20:
20:
20:
20:
21:
21:
21:
21:
21:
21:
22:
22:
22:
22:
22:
23:
23:
24:
24:
00
05
40
45
52
56
01
21
49
03
08
12
35
46
56
01
13
21
40
52
57
12
26
32
39
43
02
09
35
58
0.
RO
RO
RO
RO
RO
RO
RO
RO
RO
RO
RO
RO
RO
RO
RO
RO
RO
RO
RO
RO
RO
RO
RO
RO
RO
65-0.89
1
0
0
3
0
0
0
0
1
3
0
0
5
0
0
0
0
4
0
3
0
0
0
0
0
0
0
0
0
2
.96
.62
.83
.63
.85
.24
.47
.23
.59
.71
.43
.31
.61
.39
.97
.11
.48
.18
.25
.16
.12
.82
.47
.36
.26
.78
.44
.78
.47
.27
Peak
0:
18:
18:
18:
18:
19:
21:
21:
22:
22:
00
03
07
28
31
28
11
48
17
31
0.
RO
RO
RO
RO
RO
RO
RO
RO
2.
5.
3.
1.
2.
1.
7.
5.
6.
8.
10.
6.
1.
6.
5.
0.
11.
0.
4.
1.
0.
3.
4.
14.
1.
11.
6.
11.
4.
1.
14.
94
98
32
13
26
72
47
56
14
25
67
74
45
44
08
92
98
97
32
24
64
63
71
53
88
26
46
97
09
84
53
65-0.89
1
0
1
1
1
4
0
1
0
0
.84
.26
.89
.07
.11
.82
.59
.25
.76
.79
8.
2.
3.
4.
5.
2.
13.
6.
8.
3,272.
69
51
29
41
06
37
42
39
50
27
6.32
0.797-1.100
0.000
0.803
0.829
0.833
0.838
0.841
0.845
0.859
0.880
0.890
0.894
0.897
0.914
0.922
0.930
0.933
0.942
0.948
0.962
0.971
0.975
0.986
0.996
17.40 1.001 2378-TCDF
AN
006
009
023
028
092
1,441.48
1.109
0.955-1.045
0.000
0.802
0.805
0.820
0.822
0.865
0.941
0.968
0.990
1,830.79 1.000 13C12-2378-TCDF ISO
Triangle Laboratories, Inc.® Analytical Services Division
801 Capitola Drive • Durham, North Carolina 27713
Phone: (919) 544-5729 • Fax: (919) 544-5491
Printed: 14:58 09/12/97
101
-------
Page No.
09/12/97
Lifting of X973082B.dbf
Matched GC Peak* / Ratio
/ Ret. Time
Compound/
M_Z.... QC.Log Omit Why ..RT. OK Ratio Total.Area... Area.Peak.1.. Area.Peak.2.. Rel.RT Compound.Name.,
ID.. Flags.
316-318
13C12-TCDD
332-334
332-334
DC
DC
DC
DC
DC
DC
DC
DC
DC
DC
DC
DC
DC
SN
SK
WH
WH
WH
WH
WH
WH
WH
1
NL
SN
SN
WH
2
22:
23:
23:
24:
24:
24:
24:
24:
24:
56
14
58
00
12
18
21
31
58
RO
RO
RO
RO
RO
RO
RO
1.
0
1
3
1
0
0
1
5
.45
.45
.51
.94
.21
.87
.87
.39
.37
Peak
0:
21:
21:
22:
22:
23:
00
13
30
01
05
30
0.
RO
BO
RO
65-0.89
0
0
0
1
1
1
.84
.74
.76
.55
.83
.41
Peaka
3.72
4.78
5.86
2.21
12.83
9.69
14.15
69.76
2.41
3,272.27
Above: TCDF / TCDD Follow*
019
032
064
,066
,075
.079
.081
.089
1.109
30.92
2,790.70
3,190.90
13.81
11.47
8.87
5,981.60
0.906-1.094
0.000
1,190.85 1,599.85 1.000 13C12-2378-TCDD IS1
1,375.74 1,815.16 1.013 13C12-1234-TCDD RSI
1.038
1.041
1.108
Column Description -Why" Code Description QC Log Desa.
M_Z -NoBinal Ion Maas(es)
..RT. -Retention Time (mm:SB)
Rat.l -Ratio of M/M+2 Ions
OK -RO-Rotio Outside Limits
Rel.RT-Relative Retention Time
••• End of Report
WL-Below Retention Time Window
WH-Above Retention Time Window
SN-Below Signal to Noise Level
-------
A5.21E4
A2.80E4 » A1.88E4
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Staple TuxttI-M23-l 1X1*43057 Pi.lt Ttoctt TRIANGLE LABS
1009f A1.73X5
18x00 15*00 20<00 21(00 22'tOO 23'tOO
Pll»tZ973082 #1-1285 JLoqill-SSP-1997 21:48110 OC EH- Voltafff SIR AutoSpme Solt»t832
305.8987 BSUB<2S6,30,-3.0) PKD(S,3,1, 0.10*,3328. 0, 0. 00%,P,P) BxpiXCONP TT
Saaplf TmxttI-1123-1 TLH430S7 Pil» Tmxtt TRIANGLE LABS
10°* A1.96E5
I I I I I- 0-0*0
25 tOO Time
ISiOO 19:00 20*00 21:00 22:00 23:00 24(00
Pll»:X973082 #1-1285 Aoj:ll-SEP-lS97 21(48(10 OC SI+ Voltmff* SIR AutoSp»c Soim»t4524
315.9419 BSV3(25f,30,-3.0) tKD(S,3,l,0. 10%, 18096.0, 0.00\,P,P) BxpiXCOSP TT
Sanpl» Tuxt:I-M23-l TLIt43057 Pilf Tuxtt TRIANGLE LABS ~
JL1.J4E7
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20;
18(00 15(00 ' 20(00 ' ' ' 21:00 ' ' ' 22(00 ' ' ' 23(00 ' * ' 24(00
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A1.$3E7
ao:
40:
20:
18(00
15(00
20(00
2lo
22(00 33(00
SIR AUtoSpOC
34(00
Saoplu T«t(J-M23-l TLI*43057 Pilt Tfxtt TRIAKOLE LABS
19tS6
0.0*0
25(00 Tin*
J2.0Xf
.1.3*6
.6.7X5
.0.0*0
t-*T
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.3.5*6
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.8.7*5
.0.0*0
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22100
23100
24100
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33 tOO Tim»
103
-------
Pil»tX973082 I1-12B5 lcqill-SSP-1997 2li4B:lO CC Eli- Volt»g» SIR AutoSp«c Voii»:740
319.896S BSUB(2Sf,30,-3.0) PKD(5,3,l,0.10*,2960.0,O.OO*,P,r)
Saapl* r«rt»I-J03-l TLH430S7 Fill Tmxtt TRIUH3LX LABS
19', 00 20:00 21100 22tOO 23«00
Pil*:X973082 #1-1285 JLcq:ll-3XP-1997 21:48:10 OC XI+ Volttfff SIR JMtoSpfC Bbl««<3585
321.8936 BSUB(25f,30, -3.0) PKD(S,3,1,0.10*1,14340.0, 0.00*,r,P
Saxpl* Tuxt:I-K23-l TLIt430S7 Film Ttocti TRBWOLX LIBS
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Fil»tX973082 #1-1265 JLcqill-SSP-1997 21:48110 OC XI* Voltmgf SIR Auto5p«c Ooim»il669
327.8847 BSUB(256,30,-3.0) PKD{5,3,l,0.imr667f.O,O.OO*rFfF) ExptKOHP_TT
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100*
80J
40.
20.
A2.31B7
20*00 21(00 22(00 23:00
Pll*:X973082 #1-1285 Acqtll-SXP-1997 21(48(10 OC XI* Voltffff SIR JMtoSpma Bolm»:70SO
331.9368 BSUB(256,30,-3.0) PKD(5,3,l,0.10\f28200.0,0.00*,FfF) X*piXCOKP_TT
TmxtiI-M23-l TLI*43057 File T«urt. TRHBOLX ULBS
A1.3BX7
U.19X7
80.
40J
20.
19:00 20:00 21:00 22iOO 23<00
Fil«iZ973082 #1-1285 Acg>ll-5EP-1957 21>48>10 0C XX* Volta?* 5IH AutoSp-c «oi*«>8409
333.5338 BSUB(256,30,-3.0) PXD(5,3,1,0.10\,3363S.O,0.00\,P,P) SxpiKOHF,TT
Staple rwrtrX-103-1 TLI0430S7 File T«xt» TBXUlWLC ULBS
100H
A1.82X7
JL1.60X7 I
24100
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24(00 Tiai*
1.5X7
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.3.1X6
24100
.0.0X0
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104
-------
18tOO 19100 20:00 21(00 22<00 33tOO 24(00
•ilftX973082 91-1285 Acqtll-SBP-1997 21:48(10 OC XH- Voltage SIR AutoSp»c
319.8965 B3CptKOHP_TT
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ll»:X973082 #1-1285 Acq:ll-SEP-1997 21:48(10 OC II* Voltage SI* AuCoSpee
03.5015 Exp:XCONP_TT
euaplf Pwrt(J-M23-l TLHM3057 File T«rt( IRZUHtLE LABS
00* 20;03
80;
18(00 15(00 20(00 21(00 22(00 23(00
'il«(Z573082 #1-1285 Acgi 11-3SP-1997 21(48(10 OC XI* Voltage SIR AutoSpee
15.5415 ExpiKOUP TT
laople T«xtrI-JC3-l T£X*43057 File T»xti TKOOKLX LABS
1001
so:
40:
20:
24(00
25(00 Tin*
.2.7B6
.2.0B6
.1.3X6
.6.7BS
O.OBO
25 ( 00 Tim»
18(00 15(00 20(00 21(00 22(00
PilmiX973082 #1-1285 Aoqill-SBP-1997 21(48>10 OC ST+ Vbltag*
331.9368 ExpiXCONF_rr
I>WCt(I-M23-l T£Xf43057 Pllf Taxtt rXZAOOL* LABS
23(00
AutoSpec
24 tOO
lOOt
so:
col
40:
20:
25(00 Tim
-3.0E6
12.2X6
-.1.5X6
.7.425
O.OBO
18(00 15(00 20(00 21(00 22(00 23(00
Pll»tZ973082 01-1285 Acgtll-SBP-1997 21(48(10 OC XI* Voltag* SIR AutoSptc
293.9835 X3tptXCOSf_TT
Saaplu TvctiI-H23-l TLI*43057 Pile T«xtj TXIANOLX LABS
ion
80:
60:
40:
20:
0:
18:50
34 22,04 "L3e">01
24 tOO
24 102
25100 Tim*
^
.7.4X7
9X7
-.4.5X7
.3.0X7
.1.5*7
O.OZO
18(00 15(00 20(00 21(00 22(00 23(00 24(00
Fil«(X573082 #1-1285 Acqtll-SBP-1997 21(48(10 OC XI* Voltage SIR AutoSpto
330.9792 XxptKONP_TT
3»afl» T«ct(X-M23-l TLX#43057 Pll* Twrt( nZUOL* LABS
1009
80:
to:
40:
20:
oj
18(00 15(00 20(00 21(00 22*00 23(00 24(00
25(00
\-~-~~~^&£~~-£X2~~*~*^^^ 21'37 ^~~*&3!&&~&&J^
,8
.7
.5
.3
.1
0
0.0*0
25(00 Tim*
105
-------
CD
O
Peak Locate Examination:ll-SEP-1997:21:47 File:X973082
Experiment:XCONF_TT Function:! Reference:PFK
-------
FiIeTX973082 #1-1285 Acq:ll-SfiP-1997 21:48:10 GC'El+ Voltage Sift AutoSpec
303.9016 Exp:XCONF_TT
Sample Text:I-M23-l TLI#43057 File Text: TRIANGLE LABS
100& A6.32E4
80J
60J
40J
20J
• I 1 I I I I I I I I I I I I I I I I I I I I I I I I I I I I I I I I I I I I I I I ' T I ..... I ..... I ..... I I .... I ••
21:48 22:00 22:12 22:24 22:36 22:48 23:00 23:12 23:24 23:36 23:48 24:00
File:X973082 #1-1285 Acq:ll-SEP-1997 21:48:10 GC EI+ Voltage SIR AutoSpec
305.8987 Exp:XCONF_TT
Sample Text:I-M23-l TLI#43057 File Text: TRIANGLE LABS
24li2'24:24
5.2E4
14 . 1E4
L3.1E4
L2.1E4
L1.0E4
3.0EO
Time
100%
80 j
60 j
40J
20J
74E5
21:48 22:66 ' 22:12 ' 22: 24" 22 ! 36 ' 22: 48" 23 ! 66 ' 23:12 23-124 23!36 23:48 24:66
File:X973082 #1-1285 Acq:ll-SEP-1997 21:48:10 GC EI+ Voltage SIR AutoSpec
315.9419 Exp:XCONF_TT
Sample Text:I-M23-l TLI#43057 File Text: TRIANGLE LABS
lOOi 22;31
80J
60J
20j
8.5E4
_6.8E4
_5.1E4
_3.4E4
_1.7E4
. O.ORQ
24:12 24:24 Time
3.4E6
L2.7E6
L2.0E6
L1.3E6
L6.7E5
2lT48 22:00 22:12 22:24 22:36 22:48 23:00 23:12 23:24 23:36 23:48 24:00
i . j . . . ,-,-jP n . OEO
24:12 24:24 Time
-------
TLI Project: 43057
Client Sample: O-M23-1
Method 23 PCDD/PCDF Analysis (a)
Analysis File: S975809
Client Project ~A«.pH*cr -PUM'
Sample Matrix: M23TRAIN
TLI ID: 181-27-2A-C
Sample Size: 1.000
Dry Weight n/a
GC Column: DB-5
Date Received: 08/29/97 Spike File: SPX23704
Date Extracted: 09/06/97 ICal: SF56117
Date Analyzed: 09/10/97 ConCal: S975797
Dilution Factor, n/a % Moisture: n/a
Blank File: S975807 % Lipid: n/a
Analyst ML % Solids: n/a
^Aifwi^ss^^^!^ %T5$r$f?f8
23,7,8-TCDD
1,23,7,8-PeCDD
1,23,4,7,8-HxCDD
1,23,6,7,8-HxCDD
1,23,7.8,9-HxCDD
1,23,4,6,7,8-HpCDD
1,23,4,6,7,8,9-OCDD
ND 0.003
ND 0.005
ND 0.006
0.01
0.02
0.06
0.53
*8ftwlHT'*'JTOBr
1.24
1.29
0.99
0.91
29:13
2930
32.-04 B_
3433
23,7.8-TCDF
1,23,7,8-PeCDF
2,3,4.7,8-PeODF
1,2^,4,7,8-HxCDF
!A3.6,7.8-HxCDF
2^,4.6,7,8-HxCDF
1,2^,7,8,9-HxCDF
1,2^,4,6,7,8-HpCDF
1,23,4,7,8,9-HpCDF
1,^3,4,6,7.8,9-OCDF
0.02
EMPC
EMPC
0.04
0.01
0.02
ND
EMPC
0.04
0.04
0.81
0.006
0.01
0.004
0.07
1.36
133
1.17
0.80
20:25
28:23
28:29
29:00
32:24
34:41
B_
in
PRB
B_
PRB
FSB
B_
B
^^
-------
Project 43057
iient Sample: O-M23-1
Method 23 PCDD/PCDF Analysis (a)
Analysis File: S975809
internal Standard {a;:;;
JC«-2,3.7,8-TCDF
JC,2-2,3,7,8-TCDD
3C,rlA3.6,7,8-HxCDF
>C,2-l,2,3,6,7,8-HxCDD
JC,2-l,2,3,4.6,7,8-HpCDF
3Cu-lA3,4,6,7,8-HpCDD
3C,2-1A3,4,6,7,8,9-OCDD
2.8
25
2.7
2.7
2.8
2.6
1.7
2.0
2.9
69.4
63.2
67.1
68.2
68.8
65.4
42.3
50.4
36.0
40%-130%
40%-130%
40%-130%
40%-130%
40%-130%
40%-130%
25%-130%
25%-130%
25%-130%
0.76
0.78
1.46
1.50
0.50
1.24
0.44
1.05
0.89
20:24
21:13
24:43
25:52
28:29
29:12
31:11
32:03
34:33
7CU-2^,7,8-TCDD
3Co-2^,4,7,8-PeCDF
3C,rl,2,3,4,7,8-HxCDF
3CirlA3,4,7,8-HxCDD
3C,2-l,2,3,4,7,8,9-HpCDF
3.8
3.4
3.5
3.2
3.5
96.1
86.1
87.3
81.0
88.7
70%-140%
70%-140%
70%-140%
70%-140%
70%-140%
1.45
0.49
1.22
0.42
21:14
25:30
28:22
29:07
32:24
3C,2-l,2,3,7,8,9-HxCDF
3C12-2^,4,6,7,8-HxCDF
23
2J5
58.1
61.4
40%-130%
40%-130%
0.49
0.51
29:42
28:59
.,
..V ..
3C12-lA3,7.8,9-HxCDD
0.80
1.23
21:00
29:30
Data Reviewer.
A/V
09/11/97
Page 2 of 2
XZ3TJSKv2jOO.tAUtt.ta04
Triangle Laboratories, Inc.*
301 Capttola Drive • Durham, North Carolina 27713
3hone: (919) 544-5729 • Fax: (919) 544-5491
rtted: 14:56 09/1 1/97
109
-------
Data Review By:
Calculated Noise Area:
1.22
The Total Area for each peak with an ion abundance ratio outside
ratio limits has been recalculated according to method requirements.
Page No.
09/11/97
Listing of S975809B.dbf
Matched GC Peaks / Ratio / Ret. Ti»e
Compound/
M_Z QC.Log Oo.it why . .RT. OK Ratio Total. Area... Area. Peak. 1.. Area. Peak. 2.. Rel.RT Compound. Hue.. ID.. Flags.
TCDF
304-306
0
D
D
0
304-306
13C12-TCDF
316-318
DC
DC
DC
DC
D
D
D
DC
D
DC
DC
DC
DC
HL
SN
SN
SN
SN
SN
SN
SN
SN
SN
WH
4
HL
HL
0
16
17
17
17
18
:00
:S4
:16
:26
:41
-.29
0.
HO
RO
19:15
19
19
20
20
20
21
22
22
:31
:57
:12
:25
:56
:44
:20
:50
RO
RO
RO
RO
RO
65-0.89
1.
0.
0.
0.
0.
0.
0.
1.
0.
0.
0.
0.
1.
0.
1.
33
83
73
33
74
84
81
01
78
57
81
64
09
72
41
Peaks
0
19
19
:00
:11
:SS
0.
RO
RO
20:24
316-318
TCDD
320-322
A
DC
DC
DC
DC
DC
DC
DC
DC
DC
DC
DC
DC
3
NL
SN
SN
SN
SN
SN
SN
SN
SN
SN
SN
WH
20
:54
65-
1.
0.
0.
0.
0.
Peaks
0
18
18
:00
:19
:48
19:00
19
19
19
19
20
21
21
22
22
:13
:27
:37
:56
:23
:50
:55
:02
:09
0.
RO
RO
RO
RO
RO
RO
RO
RO
RO
RO
HO
22:16
22
:32
RO
0.89
00
99
73
76 4
67
4
65-0.89
1.
0.
0.
1.
0.
0.
0.
0.
3.
1.
2.
8.
1.
0.
2.
17
56
90
14
51
87
51
78
57
74
96
50
38
,66
.63
0
2
0
1
3
5
4
8
13
1
20
4
0
6
0
49
.11
.95
.57
.03
.67
.69
.60
.58 4.89
.28 5.82
.82
.65 9.27
.09
.96
.54 2.74
.69
.05
0.823-1.104
0.
0.
0.
0.
0.
0.
0.
4.85 0.
7.46 0.
0.
11.38 1.
1.
1.
3.80 1.
1.
000
828
846
855
867
906
944
957
978
990
001 2378 -TCDF AN
026
065
095
119
0.951-1.049
0
7
23
,405
22
.12
.19
.80 10.08
.97 1,897.60
.67 9.13
0.
0.
13.72 0.
2,508.37 1.
13.54 1.
000
940
976
000 13C12-2378-TCDF ISO
025
,452.44
0
8
6
0
0
0
0
6
1
0
0
0
0
0
0
.11
.99 3.91
.74 3.43
.50
.53
.58
.41
.67 2.93
.43
.41
.46
.07
.28
.48
.48
0.857-1.061
0.
6 . 94 0 .
000
863
3.81 0.886
0.
0.
0.
896
906
917
0.925
3.74 0.940
0.961
1.029
1.033
1.038
1.044
1.049
1.
,062
Triangle Laboratories, Inc.® Analytical Services Division
801 Capitola Drive • Durham, North Carolina 27713
Phone: (919) 544-5729 • Fax: (919) 544-5491
Printed: 14:57 09/11/97
110
-------
Page No.
09/11/97
Listing of S975809B.dbf
Matched GC Peaks / Ratio / Bet. Time
Compound/
M_Z QC.Log Omit Why . .RT. OK Ratio Total. Area... Area. Peak. 1.. Area. Peak. 2. . Rel.RT Compound. Hue. . ID.. Flag*.
320-322
3 Peaks
22.40
37C1-TCDD
328
328
13C12-TCDD
332-334
332-334
PeCDF
340-342
D
A
M
D
M
340-342
13C12-PeCDF
352-354
DC ML 0:00
DC WL 18:38
19:41
21:14
21:26
21:33
DC SH 21:41
21:42
5 Peaks
0.
DC ML 0
19
20
21
21
21
DC SN 22
:00 RO
:54
:39 RO
:00
:13
:36
:22
2.
2,
65-0.89
14.
0.
1.
0.
0.
0.
0.
5 Peaks
1.
DC NL 0:00 RO
D SN 22
DC SN 22
DC SN 22
DC SN 23
DC SN 23
23
23
24
24
D SN 25
25
25
DC SN 25
DC SN 26
26
:37 RO
:48
:53 RO
:06 RO
:11 RO
:50
:59
:27
:44 RO
:02 RO
:30 RO
:39
:57
:05 RO
:21 RO
32-
1.
1.
1.
4.
0.
0.
1.
1.
1.
1.
1.
1.
1.
1.
1.
2.
00
79
80
80 4,
78 3,
83
79
8,
1.78
00
20
76
36
14
56
56
53
33
88
18
11
55
44
23
19
7 Peaks
DC NL 0
23
24
24
25
25
26
1.
:00 RO
:48
:22 RO
:43
:03
:30
:29 RO
32-
1.
1.
1.
1.
1.
1.
2.
1.78
14
33
20
46 3,
40
45 3,
22
0.07
1.02
13.99
629.87
5.05
5.28
1.24
3.65
657.84
0.14
21.85
2.89
818.59
245.44
56.81
3.12
145.58
TCDD /
0.12
5.43
0.47
0.36
0.23
0.31
15.18
7.33
14.78
6.27
5.89
9.28
9.27
3.08
1.07
4.67
66.78
0.13
16.12
14.05
661.64
24.31
058.59
7.85
13
2,629
5
S
3
9
3
2,143
1,421
25
.99
.87
.05
.28
.65
.61
.93
.61
.01
.81
12.
1.
2,674.
1, 824 .
31.
0.
0.
24
63
98
43
00
906-1.094
0.000
0.878
0.928
1.001 37C1-TCDD
1.010
1.016
1.022
1.023
906-1.094
0.000
0.938
0.973
0.990 13C12- 1234 -TCDD
1.000 13C12-2378-TCDD
1.018
1.054
StJRl
RSI
IS1
9
4
8
4
5
5
4
9
8
2,170
14
1,808
6
.25
.43
.45
.62
.64
.64
.00
.21
.54
.84
.18
.68
.84
5.
2.
6.
2.
5.
3.
1.
6.
7.
1,490.
10.
1,249.
3.
0.
93
90
33
46
06
63
83
0.
91
11
80
13
91
08
909-1.079
0.000
0.915
0.922
0.926
0.935
0.938
0.964
0.970
0.989
1.001 12378- PeCDF
1.013
1.032 23478-PeCDF
1.038
1.050
1.055
1.066
838-1.162
0.000
0.963
0.986
1.000 13C12- PeCDF 123
1.013
1.032 13C12- PeCDF 234
1.071
AN
AN
IS2
SOR2
Triangle Laboratories, Inc.® Analytical Services Division
801 Capitola Drive • Durham, North Carolina 27713
Phone: (919) 544-5729 • Fax: (919) 544-5491
Printed: 14:57 09/11/97
. Ill
-------
Page No.
09/11/97
Listing of S975809B.dbf
Matched GC Peaks / Ratio / Ret. Time
Compound/
M_Z.... QC.Log Omit Why ..RT. OK Ratio Total.Area... Area.Peak.1.. Area.Peak.2.. Rel.RT Compound.Name.. ID.. Flag*.
352-354
PeCDD
356-358
356-358
13C12-PeCDD
368-370
368-370
BxCDF
374-376
374-376
13C12-HXCDF
384-386
6 Peaks
6,782.56
DC
DC
DC
DC
DC
DC
DC
DC
DC
DC
D
D
D
D
DC
DC
DC
DC
DC
DC
DC
DC
DC
DC
NL
SN
SN
SN
SN
WH
WH
3
NL
2
NL
SN
SN
SN
SN
SN
SN
SN
SN
SN
SN
WH
WH
WH
6
NL
SN
0:00
23:59
24:21
24:45
25:04
25:43
25:52
26 : 21
26:39
26:47
Peaks
0:00
25:52
26:00
Peaks
0:00
27:24
27:32
27:41
27:49
27:58
28:23
28:29
28:35
28:47
29:00
29 : 07
29:17
29:32
29:38
29:42
29:49
30:00
30:13
30:18
Peaks
0:00
27:31
28:22
1.
RO
RO
RO
RO
RO
RO
- ADOVe :
r / reuuu to.ij.ows ---
32-1.78
1.
0.
2.
1.
00
54
37
84
2.55
0.24
1.41
RO
RO
RO
0.62
0.08
1.81
0.
7.
0.
9.
5.
0.
3.
1.
10
73 4.70
89
72 7.00
74 5.74
28
67
53
0.10
0.41
0.921-
•1.026
0.000
8.71 0.927
0.941
3.81 0.957
2.25 0.969
0.994
1.000 12378- PeCDD
AN
1.019
1.030
1.035
23.19
1.
RO
32-1.78
0.86
1.50
1.46
1.
RO
05-1.43
2.92
1.27
1.20
RO
0.89
1.35
RO
1.60
1
.32
1.36
RO
RO
RO
RO
RO
RO
RO
0
RO
RO
1
1
1
1
3
1
2
2
1
0
1
1
.22
.77
.33
.06
.00
.85
.87
.77
.24
.18
.45
.26
0.10
2,086.84 1,253.47
204.01 121.24
0.845-1.155
0.000
833.37 1.000 13C12- PeCDD 123
IS3
82.77 1.005
2,290.85
0.85
10.74 6.01
21.58 11.75
1.32
3.71
4
31
15
4
4
16
0
0
1
0
1
6
0
0
0
103
.59
.94 18.17
.18 8.76
.04
.52
.89 9.65
.99
.18
.03
.52
.46
.79 3.76
.11
.69
.70
.12
.43-0.59
0
0
0
.68
.33
.49
2
4
2,209
.14
.20
.82 722.29
0.957-1.053
0
4.73 0
9.83 0
0
0
0
13 . 77 0
6.42 1
1
1
7.24 1
1
1
1
1
1
3.03 1
1
1
1
.000
.962
.967
.972
.977
.982
.996 123478-HxCDF
.000 123678-HxCDF
.004
.011
.018 234678-HxCDF
.022
.028
.037
.040
.043 123789-KxCDF
.047
.053
.061
.064
AN
AN
AN
AN
0.859-1.141
0
0
1,487.53 0
.000
.966
.996 13C12-HXCDF 478
SOT
PR
PR
Triangle Laboratories, Inc.® Analytical Services Division
801 Capitola Drive • Durham, North Carolina 27713
Phone: (919) 544-5729 • Fax: (919) 544-5491
Printed: 14:57 09/11/97
112
-------
Page No.
09/11/97
Listing of S975809B.dbf
Matched GC Peaka / Ratio / Ret. Time
Compound/
M_Z QC.Log Omit why ..RT. OK Ratio Total.Area... Area.Peak.1. . Area.Peak.2.. Rel.RT Compound.Name.. ID.. Flaga.
384-386
HxCDD
390-392
D
390-392
13C12- HxCDD
402-404
402-404
HpCDF
408-410
M
408-410
13C12-HpCDF
418-420
28
DC SN 28
28
DC SN 29
29
29
DC SN 30
:29
:45
:59
:30
:42
:S6
:17
RO
RO
RO
RO
0.
0.
0.
0.
0.
1.
0.
5 Peaks
DC NL 0
DC HL 27
27
28
DC SN 28
28
DC SN 28
DC SN 29
D SN 29
29
29
DC WH 29
:00
:45
:54
-.23
:27
:36
:45
:00
:08
:13
-.30
:59
1.
RO
RO
RO
RO
RO
RO
50
31
51
80
49
20
28
05-1.43
0.
0.
1.
1.
2.
1.
1.
7.
1.
1.
1.
0.
19
29
21
13
59
20
94
03
22
24
29
91
5 Peaka
DC NL 0
28
29
29
29
29
DC SN 29
:00
:36
:07
:12
:30
:43
:58
1.
RO
RO
RO
2,639.
2.
2,178.
1.
1,792.
2.
0.
14
96
85
84
82
61
89
8,823.24
i HxCDF /
0.
0.
5.
30.
1.
14.
1.
0.
3.
7.
9.
3.
67.
16
18
95
36
79
79
61
74
48
72
13
09
95
876
734
589
2
.59
.47
.87
.07
1,762.55 1.000 13C12- HxCDF 678
1.009
1,444.38 1.018 13C12- HxCDF 234
1.036
1,202.95 1.043 13C12- HxCDF 789
1.73 1.051
1.063
IS4
ALT2
ALT!
3
16
8
4
5
.26
.11
.06
.27
.14
05-1.43
1.
1.
1.
1.
1.
1.
3.
5 Peaks
DC NL 0
31
31
31
DC SN 31
DC SN 32
32
DC WH 32
DC WH 32
:00
:12
:26
:33
:44
:14
:24
:42
:51
0.
RO
RO
RO
RO
RO
RO
RO
RO
10
52
22
24
23
44
40
88-1.20
23.
1.
1.
1.
2.
1.
1.
6.
2.
14
39
47
22
33
78
17
03
00
4 Peaks
DC NL 0
:00
0.
RO
1.
6.
1,631.
2,071.
3,184.
8.
2.
72
74
57
02
06
98
15
6,902.37
: HxCDD /
0.
31.
7.
10.
0.
0.
12.
0.
1.
61.
14
62
02
02
67
73
93
73
04
59
4
897
1,145
1,756
5
.57
.42
.28
.61
.76
0.951-1.015
0.000
0.950
2.69 0.955
14 . 25 0 . 972
0.974
6.73 0.979
0.985
0.993
0.998 123478-RxCDD
3.45 1.001 123 678 -HXCDD
3.99 1.010 123789-HXCDD
1.027
0.966-1.034
0.000
3.01 0.979
734.15 0.997 13C12-HXCDD 478
925.74 1.000 13C12- HxCDD 678
1,427.45 1.010 13C12-HXCDD 789
4.01 1.018
1.026
AN
AM
AM
SOR4
185
RS2
21
5
6
6
.60
.05
.01
.98
37-0.51
0.
88
1.
40
0.995-1.045
0.000
15.50 1.001 1234678-RpCDF
3.44 1.008
4.91 1.012
1.018
1.034
5. 95 1.039 1234789-HpCDF
1.049
1.053
0.936-1.128
0.000
AN
AH
Triangle Laboratories, Inc.® Analytical Services Division
801 Capitoia Drive • Durham, North Carolina 27713
Phone: (919) 544-5729 • Fax: (919) 544-5491
Printed: 14:57 09/11/97
113
-------
Page No.
09/11/97
Listing of S975809B.dbf
Matched GC Peaks / Ratio / Ret. Time
Compound/
M_Z.... QC.Log Omit why ..RT. OK Ratio Total.Area... Area.Peak.1.. Area.Peak.2.. Rel.RT Compound.Name. . ID.. Flag*.
418-420
HpCDD
424-426
424-426
13C12-HpCDD
436-438
436-438
OCDF
442-444
442-444
OCDD
458-460
458-460
DC
DC
DC
DC
DC
DC
DC
DC
DC
DC
DC
DC
DC
DC
DC
DC
DC
DC
DC
DC
DC
DC
DC
DC
DC
DC
DC
SN
2
NL
WH
2
NL
SN
1
NL
SN
SN
SN
SN
SN
SN
SN
SN
SN
SN
SN
SN
SN
SN
SN
SN
SN
SN
1
NL
SN
SN
1
31:11
31:29
32:24
Peaks
0:00
31:28
32:04
32:32
Peaks
0:00
31:26
32:03
Peak
0:00
30:43
31:07
31:35
31:51
32:13
32:18
32:51
32:58
33:33
33:59
34:08
34:11
34:21
34:41
34:59
35:10
35:23
35:31
35:49
Peak
0:00
34:22
34:33
34:49
Peak
RO
0.
RO
0.
RO
RO
0.
RO
RO
RO
RO
RO
RO
RO
RO
RO
RO
RO
RO
RO
RO
RO
RO
RO
RO
0,
RO
RO
0.44
0.22
0.42
88-1.20
1.00
1.09
0.99
2.00
88-1.20
2.00
2.97
1.05
76-1.02
1.40
0.27
1.06
0.83
0.24
3.44
1.76
0.74
0.38
4.78
3.53
1.15
1.40
1.18
0.80
0.18
2.52
1.35
0.71
0.74
.76-1.02
0.86
2.17
0.91
1.49
1,194.47
2.00
816.94
2,011.41
: HpCDF /
0.14
16.15
19.94
0.27
36.09
2.16
3.08
1,307.85
1,307.85
• Hrw"nri /
: tipv^uu /
0.09
0.15
0.32
1.48
0.17
0.30
0.72
1.40
0.59
0.17
0.32
0.89
0.19
0.76
9.20
0.66
0.40
1.42
0.72
0.30
9.20
0.13
0.45
86.40
0.96
86.40
670.48
AN
0.969-1.031
0.000
0.981
637.37 1.000 13C12-HpCDD 678 IS?
Follows
4 . 10
0.884-1.116
0.000
0.889
0.901
0.914
0.922
0.932
0.935
0.951
0.954
0.971
0.984
0.988
0.989
0.994
5.10 1.004 OCDF
AN
,013
018
,024
,028
41.23
1.037
0.884-1.116
0.000
0.995
45.17 1.000 OCDD
1.008
AN
Triangle Laboratories, Inc.® Analytical Services Division
801 Capitals Drive • Durham, North Carolina 27713
Phone: (919) 544-5729 • Fax: (919) 544-5491
Printed: 14:57 09/11/97
114
-------
Page No. 6 Listing of S975809B.dbf
09/11/97 Matched GC Peaks / Ratio / Ret. Time
Compound/
M_Z QC.Log Omit Why ..RT. OK Ratio Total.Area... Area.Peak.1.. Area.Peak.2.. Rel.RT Compound.Name.. ID.. Flags.
13C12-OCDD 0.76-1.02 0.996-1.005
470-472 DC NL 0:00 RO 9.50 0.11 O.OOO
34:33 0.89 1,190.52 560.85 629.67 1.000 13C12-OCDD IS8
DC WH 34:52 RO 0.14 0.53 1.009
470-472 1 Peak 1,190.52
Column Deacription "Why* Code Description QC Log Deso.
M_Z -Nominal Ion Mass(ea) HL-Below Retention Time Window A-Peak Added
..RT. -Retention Time (mm:as) WH-Above Retention Time Window R-Peak Kept
Rat.l -Ratio of M/M+2 Ions SN-Below signal to Noise Level D-Peak Deleted
OK -RO-Ratio Outside Limits
-------
±l*sS975809 #1-040 AcqtlO-SXP-1997 21:48:09 EI+ Voltag* SIX 703 Koit»:41
03.9016 T:2 BSOB(256r30r-3.0) PKD(9, 5,5, 0.05\, 164.0,1.00*,r,T) XxpiXPCUS
TRIANGLE LABS Tf*tiO-M23-l 1X1*4.3057 IKT. TIME - 21:50
1004 A9.27E4
17tOO 10:00 15:00 20tOO 21tOO
r±l»:3975809 #1-840 Acq: 10-3XP-1997 21:48,09 XI* Volt*gm SIS 70S Boil*132
305.8987 ft2 BSOB(256,30,-3.0) PKB(9, 5,5,0.05\,128.0,1.00\,F,T) XzptXPCUS
TSIAHBLE LABS T*Xt.:O-M23-l TLH43057 ZJKT. TUB - 21:50
1004 A1.14XS
17:00 10(00 19:00 20(00 21(00 22(00
JTila: 55 75005 #1-848 Acq:10-SXP-19S7 21(40:05 EI+ Volt*g» SIS 70S Holm* ,35
315.9419 r,2 BSOB(256f30,-3.0) PXD(9,5,5,0.05%,140.0,1.00\,r,T) XxptXPCUS
TRIANGLE LABS T*xtiO-M23-l TUH3057 XJKT. TIMX - 21:50
1004 A1.90X7
50:
40:
201
OJ
22100
4.
-.3 .
-.2.
-.1.
.9.
.0.
17(00 18iOO 15(00 20(00 21(00
File:S975S09 H-848 AcgilO-SXT-1997 21:48t09 XI+ Voltagm SIS 70S Soil* 1 37
317.9389 T:2 BSUB(256,30,-3.0) PKD(9r5,5,0.05\,148.0,1.00\,T,T) ExptEPCOS
TRIANGLE LABS TextsO-H23-l TLH43057 IXT. TOtX - 21(50
1004
00J
40
20J
22tOO
17:0010:00 15(00 SOsOO 21(00 22(00
rile:S975809 #1-848 AcqtlO-SXP-1997 21:40:05 £X+ Voltage 5XJt 705
330.9792 Ts2 XxpiEPCOS
TRIANGLE LABS rext:O-M23-l TLI#43057 IKT. TIME - 21:50
20:50 21*43
0.
5X6
6X6
7X6
8X6
0X5
0X0
0X6
8X6
6X6
4X6
2X6
0X0
22:36
211 00
17:00 10:00 15(00 20(00
ril»:S975809 41-040 Acq:10-SZP-1997 21:48:09 ZI+ Voltage SIS 70S
375.8364 r>2 XxptXPCOS
TXIANGLX LABS Taxt:0-M23-l XLH43057 IXT. TIMX -
1004 30 38
22:00
21150
00:
50:
40:
20:
o:
17>03
'l7(00
1S\2S ,a f, 19,27
. 18:45 i
I I I I i 20:10 L
_^WIU-JLL>-4-^^
'l0(00 ' ' ' 15loo' ' ' ' '20:00'
21,« »jH
^Jl^JLJidLuAAju^
21:00
22:00
.5X6
.4X6
.3X6
.1X6
.0X0
Tim*
.3X4
.0X4
.6X3
.1X3
.5X3
.0X0
Tim
116
-------
ril*:S975809 #1-848 AcgtlO-SXP-1997 21:40:05 EI+ Voltage SIX 70S Noif*:37
319.8965 Ti3 BSOB(256,30,-3.0) PXD(7,5,3,0.05\f148.0,1.00\,r,T) ElptEPCUS
TSI ANGLE LABS T*zttO-M23-l TLH43057 IJKT. TZHX - 21:50
1001 A3. 3X4
22:00
19i00 20tOO 21:00
fil*:S975809 #1-848 Acq:10-SEP-1997 21:48:09 XI+ Voltage SIX 70S Nairn*t32
321.8936 T:2 BSUB(256,30,-3.0) PXD(7,5,3,0.05\,128.0,1.00\,T,T) ElptEPCUS
TRIANGLE LABS T*xtsO-K23-l TLI4430S7 XK7. TIME - 21:50
100J
80:
60:
20:
A3.81E4
A3. 74*4
*3'3*3
A
A4.76E4
A3.69E3
1.06X4
^2.3X4
-.1.9X4
.1.4X4
.9.4*3
.4.7X3
:±
*f*
if-
15:00 20:00 21:00 22:00
ril*iS975809 #1-848 AoqtlO-SXP-1997 21:48<05 £1+ Voltage SIX 70S SoifmtSSO
331.9368 T:2 BSUB(256,30,-3.0) PXD(7,5,3,0.05\,2240.0,1.00\,T,T) XrptXPCUS
TRIANGLE LABS T*xt.:O-H33-l TLH43057 X2KT. TIME - 21:50
100J
80:
20:
nA^ru^i*^ ^ 1
FVrl) n~
22iOO
15:00 20:00 21:00
Fil«tS975809 #1-848 AoyslO-SXr-1997 21t48t09 SI+ Voltage SIX 70S No±t»:38
333.9338 Ts3 BSU3(356,30,-3.0) PXD(7,5,3,0.05\,152.0,1.00\,r,T) XxpiXPdTS
TRIANGLE LABS TmrtsO-M23-l TLH430S7 UKT. TIME - 21:50
1004 A3.67X7
00:
60:
40:
20:
o:
Al.82X7
19:00 20:00 21:00
riletS975809 #1-848 AoqtlO-SXP-1997 21:48:05 EH- Voltage SIX 70S Ooi**i34
327.8847 T:2 BSUB(356,30, -3. 0) PKD(7,5,3,0.05\,136.0,1.00\,r,T) XzptEPCUS
TRIANGLE LABS rext.-O-M2.3-l TLI#43057 UfT. TXMf - 21:50
100J
80:
60:
40:
20:
o
A2
15:00 20:00 21:00
rilm:S975809 #1-848 AcytlO-SXP-1997 31:48:09 EH- Voltage SIX 70S
330.9792 T:2 XxptCPCUS
TRIANGLE LABS T*xttO-M33-l TLI#43057 XIK7. TIME
100J
80:
20:
OJ
22:00
21:50
19:00
20:00
21:00
22:00
jrraxo
Tim*
,5.5*6
.4.4*6
.3.3X6
.2.3X6
.1.1*6
0.0*0
Tim*
-6.8*6
.5.4X6
.4.1*6
.2.7*6
-1.4X6
0.0X0
Tim*\
6.8*6
.5.4*6
.4.1*6
.2.7*6
.1.4*6
0.0X0
Tim*
^5.7X6
.4.5X6
.3.4X6
.2.3X6
.1.1X6
0.0X0
Tim*\
117
-------
'3.1»,S975B09 H-848 AoqtlO-SXP-1997 21.148:09 XI+ VoltMyf SIX 70S Koimm,34
339.8597 Ft2 BSUB(256, 30, -3. 0) HO>(7,5,3,0.051,136.0,1.00\,r,T) XiptXPCUS
TRIANGLE LABS T*xtiO-H23-l TLH43057 HKT. TIHX - 21i50
A9.25S4
55:00
33.00 24,00 25100
r±l»,S975B09 H-848 AoqtlO-SSP-1997 21t48t09 JCT+ Voltag* SIX 70S Boim*t33
341.8567 T>2 BSVB(256,30,-3.0) PKD(7,5,3,0.05\,132.0,1.00\,r,T) ExptXPCUS
XXIAHGLX LABS Text,O-M23-l TLH43057 IXT. TIMS - 21t50
lOOi. A6.33X4
26100
23,00 24,00 25,00
Til»,S975B09 fl-848 AcqtlO-SXP-1997 21,48,09 XH- VoltMgm SIX 70S Soifm,38
351.9000 Ti2 BSOB(256,30,-3.0) PKD(7f5,3,0.05\,152.0,1.00\,r,T) XxptXTCUS
TXIAWSLX LABS TmitiO-H23-l TLH43057 UKT. TIKE - 21.50
1001 A2.17X7
so
601
40:
20.
1.81X7
26100
23,00 24,00 25,00
F±l*iS975809 fl-848 AcqilO-SXT-1997 21t48t09 XH- VoltMgm SIX 70S Soim«t36
353.8970 Ti2 BSOB(256,30,-3.0) PXD(7,5,3,0.05\,144.0,1.00\,T,T) XscpiETCUS
TSIANSLE LABS T«JCt,O-H23-l TLH43057 OKT. TIMS - 21,50
1001 A1.49E7
SOj
sol
401
201
A1.2SS7
I V.
.6.6X6
.5.3X6
.4.0X6
.2.6X6
.1.3X6
.0.0X0
line
.4.5X6
.3.6X6
.2. 7X6
.1. 8E6
.9.1X5
23,00 34,00 25,00 26,00
Tile,S975809 fl-848 Acq>10-SXP-1997 21,48,09 XI+ Volt*y» SIX 70S
330.9792 T:2 XxptXPCBS
TMIAKSLE LABS T*xt:O-M23-l TLH430S7 HKT. TIME - 21:50
23,54 24,23 25,00 25,22 25j45, 26,10
.0.0X0
Tim.
1001
eol
601
401
20l
22,59
26,47
26100
23,00 24,00 25,00
ril»,S975809 tl-848 AcqtlO-SXP-1997 21,48,09 ZI+ Voltffff SIX 70S
409.7974 T:2 XxpiXPCUS
TXIANGLX LABS T*rtiO-H23-l TLH43057 UU. TIHX - 21,50
6.1X6
4.9X6
3. 7X6
,2.5X6
.1.2X6
.0.0X0
Time
23100
24100
25 tOO
26,00
118
-------
fuetsyjsson #i-B48 Acgtio-SEP-iss? 21,48,09 EI+
Voltage SIS 70S #olf*,J9
355.8546 Fi2 BSUB(256, 30, -3.0) PKD(7, 5, 3, 0.051,116.0,1. 00\,f,T) XxptXPCUS
TXIASGLX LABS T*XtsO-M23-l TLH43057
1001
80.
60.
40.
20.
• o.
A7.00E4
I A5.74E4
1
A4.70E4 I
A 11
WY vAw^->JiA*V^y LAw v'A
24tOO ' ' 25 1 00
Fil*tS975a09 tl-848 AcqilO-SXP-1997 21,48,09 XI+
UKT. TIME -
A2.1SE4 .g
vwLrWAv *r \ J* v_^
2«»00
Voltage SIX 70S Holt* ,32
21.50
ANAVJf\A_ AA~/v >vA.
-2.6E4
.3.1X4
.1.6X4
.1.1X4
.5.3X3
' 0.0 SO
Tl»e
357.8516 r:2 BSUS(256, 30, -3.0) PKD(7 ,5,3,0 .05\,128. 0,1. 00\,T,T) ExpiEPCUS
TXIASGLX LABS T*xt,0-M23-l TLH43057
1001
80.
601
'
401
•
201
A8.71E4
J
1 A3.S1E4
I \ A2.07E4 h
11 H l\ A2.25X4
A. / L lit. A
*J \ -/tA / / ^ J 'VU
"^N. 24.00 ' 25*00
ril*tS975a09 tl-848 AcqtlO-SXf-1997 31,48,09 XH-
OKT. TIMX -
21*50
A7.05X3 AS. 42X3
1 Al . 52X4 [
B Af.OSKJ A/l 1
^li-X^yA— -JVV .Aftfr
26,00
Voltage 5XJt 705 «oi*e»JO
a I 4 o r4 1
A A A A7.6&E3
rr^rrxVAArLArwAJueA^
-3.4X4
.3.0X4
'.1.5X4
.9.8X3
.4.9X3
n»e
367.8949 Ii2 BSUS(256r30,-3.0) PO}( 7 ,5,3,0 .05\,120.0, 1.00\,T,T) XxpiXTCOS
TRIANGLE LABS T*xtiO-M23-l TLH430S7
1001
80.
601
401
201
'.
01
24 , oo asToo
ril*tS975809 tl-348 AcqtlO-SEP-1997 21,48,09 XH-
IKT. TIHX •
A1.25Z7
/ Il.21f0
; \y\
20*00
Voltage SIX 70S tfoit*,35
21*50
-4.2X6
.3.4X6
.3.5X6
.1.7X6
.8.4X5
Tim*
369.8919 r,2 BSUB(2S6r30,-3 .0) PKD(7,5,3,0.05\r140.0,l~.00*rr,T) ExptXPCUS
TXIAJKLX LABS T*XttO-M23-l TLH43057
1001
80.
60.
40.
20.
0.
24 ', 00 25*00
ril*:S975809 tl-848 Acq: 10 -SEP -1997 21:48,09 XT*
330.9792 r,2 ExpiEPCUS
TXIAHGLX LABS T*XttO-M23-l TLH430S7
1001
80.
60.
40.
20.
01
23tS4 24:23 24t36 ._ 25*00
<^-^^^N _A>». _<-<^-^^s^^ ^NA-s/^~^> W/V^—V ^
V^^vy^^ ~v\/'»~>' \^ >/ ' ^. f*
\j
24 tOO 25iOO
IKT. TIMX '
A8.33E6
I
1
/ U0.2U5
/ ly\
2ff>00
Voltage SIX 70S
IXT. TIMX m
Sit 50
-3.8X6
.2.2X6
.1.7X6
.1.1X6
.5.5X5
Tim*
21 1 50
25t23 25J*5 26ilO
^>VN^V/XNX^^>~V^V\/N-VN/^ A*A *^ /V—^WA^
2ff>00
V *vv V* *
r6.1X6
.4.9X6
.3.7X6
.2.5X6
-1.2X6
Mae
119
-------
ril*,S975809 tl-405 AcqilO-SEP-1997 21:48:09
373.8208 T:3 BSOB(2S6,30,-3
TRIANGLX LABS
100S
80:
60:
40:
20:
T»JCt:0-M23-l
EI+ Voltmyt SIX 70S Moif*t557
.0) PKD(7,5,3,0.05\,2228.0,1.00\,F,T) XxpiXTCUS
TLIt43057
Al . 82X5
a
IKT. TIHX -
A1.17X5 H
A6.01E4\
AJ
' V /
27\24
'I
I A2.13X4
v, _J"V
A
29X4 \ k
1 \l\
NL^ju-J v\
A9.
A3. 57X4 1
» -2«u * ^
*•}£** J\\ J
65X4
I.
t\
21:50
-5.8X4
A1.80X4
.4.7X4
.3.5X4
.2.3X4
.1.2X4
271: 36 27\48 28'tbb 28112 28': 2 4 28': 36 28:48 29:66 29:12 29': 24 29:36 29:48 30:66 30:12 Urn*
Til*,S975809 tl-405 Acq:10-SXP-1997 21:48:09
EI+ Voltay* SIX 708 Voim*,192
375.8178 f:3 BSOB(256,30,-3.0) PXD(7, 5, 3,0. 051,768. 0,1.00\rf,T) XxptXPCOS
TRIANGLE LABS
ion
80:
eo:
40:
20:
A9.
A4 . 73X4
A
j\ I
27:24
T*zt:0-M23-l TLIt43057
83X4
A.
A1.38X5
I
1
I
A7
UKT. TIHX -
.24X4
ifU A
.A. **"t'3*? ^'"1
Ij^. »k» P
\
21:50
A3. 03X4
A
.5.5X4
.4.4X4
.3.3X4
.2.2X4
.1.1X4
• n nm-n
27:36 27:48 28:00 28,12 28:24 28:36 28,48 29:00 29,12 29,24 29,36 29,48 30,00 30,13 Tim*
Fil*,S975809 tl-405 Acq>10-SXP-1997 21:48,09
EI+ Voltagm SIX 70S maim* ,479
383.8639 T:3 BSVB(2S6,30,-3.0) TXD(7,5, 3,0.05\,1916 .0,1. 00\,F,T) XxptXTCOS
TRIANGLE LABS
1001
80:
60:
40:
20:
27:24
Fil*,S975809
385.8610 T:3
TRIASGLX LABS
100}
80.
60:
40:
20:
OJ
Taxt,O-H23-l TLIt43057
A8.77
1 ft
n
/ V '
27Y36"27\48"28Yoo"2a\i2 28:24
tl-405 Acq:10-SEP-1997 21:48,09
X6
A7.
^ J
OU. TIHX -
34X6
I
1
V
21:50
-3.2X6
AS. 90X6
A
I
/ V
12.6X6
.1.9X6
.1.3X6
.6.5X5
0.0X0
28,36 28Y48 29:66 29:12 39i24 29,36 29:48 30:66 3 6': 12 Tim*
EI+ YoltMg* SIX 70S Boif*,710
BSUB(256,30,-3.0) PKD(7, 5,3,0 .05\, 2840 .0,1. 00\,r,T) XxpiXfCUS
T*xt,0-H23-l TLH43057
UKT. TIHX - 21,50
A1.J6X7
27:24
Fil*:S975809
392.9760 T:3
A A
A
/ V
2 ?': 3 6 27\4B 28:66 2 a': 12 28:24
tl-405 AcqilO-SXf-1997 21:48:09
Xxp:XPCUS
Al.
I ]
44X7
A
I
V
A1.20E7
A
; V
6. 6X6
.5.3X6
.4.0X6
.2.6X6
-1.3X6
0.0X0
28\36' 28* M' 29:66' 29:12 29:24 29:36 29:48 30:66 30:12 Tim*
XI* Voltag* SIX 70S
XXIANGLX LABS T*xt:O-H23-l TLIt43057
ion
80:
60:
40.
20.
0
27:26 27:45
v*f~y/*^v*'^'S-/V4_/AxA^/*N^ • i-A— W
rf\Y^' ~ *>/•¥"• ^^^
28\66 28':12 2 a': 24
•^^<\^~•V - - • v
XK7. TIHX - 21:50
29,02 29:14 29:26 29:49 30,07
k._AA*A.»/^*AX\ >.W*^VJI /\A.* -.«MA/A..*./\^-A- JWV^V*^*
^v^^^y^* v^
« • — »v^ y T^yTr» Y * ^*» *
-2.8X6
'•.2.2X6
.1.7X6
.1.1X6
.5.5X5
•o.oxo
izaiji'ifliia'iiioo' 39',i2 29': 24 29': 36 29': 4 a 30\oo 30': 12 rim*
tl-405 Acq,10-SXP-1997 21,48:09 XI* Voltxya SIS 70S
Exp, XTCOS
TRIANGLE LABS X*xt:O-H23-l TLH43057
100>
80.
60.
40.
20.
0
Ajlul
27': 24
j
||7«3tf ;
MnJB. A ..A A
iB'l/I'vv/wuJU
27't36 27:48
HKT. TIHX '
21:50
30 00 -4.6X3
28,56 39 22
28,14
'.58 1 k
JL A AM)JUJ
J>vLJV«AvJu v
j
1 29:10
11 1
JuUk^j
V/1 LJ^v" ^.i^r
.
I 29,38 30,11
Li 1 1 A l
M/iv nJiH JtniJuy) JIAIL|\J]
UV IWJuVUlUI IWUWUvAOw
.3.7X3
.2.8X3
.1.8X3
-.9.2X2
•o.oxo
28':36' 28':48"29':66 29,12 29:24 29': 36 29,48 3 6': 66 3 6': 12 MM
120
-------
7IIS-
389.
TRIA1
1003
801
601
401
20.
0.
rile
391.
TRIA
1003
801
601
401
201
,$975809 U-405 Acq,10-SSf-l997 31,48, OS EI+ Voltage SIX 70S Soime,4B
8155 T:3 BSOB(256,30,-3.0) PKD(7, 5, 3,0. 051,184. 0,1.00\,r,T) XxptXTCDS
WSLE LABS Text,0-M23-l TLI*43057 UtJ. TOtX - 21i50
A1.61E5
|
II
1 \ A8.06S4
A3.26E4 \ f\ A4.26X4 AS. 14X4
IA A6.94X3 I \A^ / \JU.40W . A /\ /A A1.50X4
AJ V /V,,_A A J Y^\W VA^AW AY^^-T^ >~^ V^w^. A_/ V A__V"/VNA^|,-I fty
17,48 28:00 28,12 28': 24 2a',36 28,48 29': 00 29:12 29,24 29:36 29:48
,S975809 41-405 AcqilO-SXP-1997 21,48,09 EH- Voltage SIX 70S HOiie:234
8127 r,3 BSUB(256,30,-3.0) PKD(7,5,3,0.05\,936.0,1.00\,r,T) XxptXTCUS
NGLE LABS TextiO-M23-l TLH43057 XK7. TIMS - 21,50
Al . 42E5
|
A6.73E4
A A3. 99X4
A2.69S4 \ /V A3. 45X4 11
A / L y/ \ -jjij «i j/ A A
27:48 27,00 28:12 28\24 28t36 28,48 29': 00 29:12 29', 24 29\36 29,48
ril»iS975809 11-405 AcqilO-SEP-1997 21:48:09 EH- Voltage SIX 70S BoiMe,449
401.8558 rt3 BSUB(256,30,-3.0) PKD(7,5,3,0.05\,1796.0,l.OO\,T,T) XffiXPCOS
TRIANGLE LABS Text,O-M23-l TLH43057 HKT. TIMS - 21:50
1004 A1.76X7
801
601
40.
201
0'
Tile
403.
TRIA
1003
801
601
401
201
0'
rile
392.
TRIA
1003
801
60.
401
201
0'
A1.15X7 I
A
3?': 4 8 28'i6o 28 1 12 28\24 28\36 28\48 29\i>0 29': 12 29,24 29\36 29', 4 8
,3975809 H-405 AcqilO-SXP-1997 21,48,09 EI+ Voltage SIX 70S Boiae>409
8529 F>3 BSUB(2S6,30,-3.0) PKD(7,5,3,0.05\,1636.0,1.00\,r,T) XxpsEPCUS
MGLE LABS Text,O-M23-l TLH43057 IXT. TIME - 21 ,50
A1.43X7
A
T
A
Ivl H
27': 4 8 28,00 28,12 28,24 28\36 28\48 29:00 29,12 29\24 29,36 29:48
,5975809 tl-405 AcqilO-SEP-1997 21,48,09 EH- Voltage SIX 70S
9760 F,3 XxpiXPCOS
jfSLE LABS Text,0-M23-l TLH43057 XK7. TIME • 21:50
*^J^t«>/V**$*tf^^
77(48 28:00 28': 12 28': 34 2»\36 28\48 29:00 29', 12 29', 24 29,36 29\48
.6.1X4
.4.9X4
.3 . 6X4
.2.4X4
.1.2X4
'0.0X0
.5.3X4
.4.2X4
.3.2X4
.2.1X4
'.1.1X4
l-
Time
-6.7X6
.5.3X6
.4.0X6
.2.7X6
.1.3X6
0.0X0
Timer
-5.2X6
.4.2X6
.3.1X6
.2.1X6
.1 . 0X6
0.0X0
Time
{.2.8X6
£.2.2X6
.1 . 7X6
.1.1X6
.5.5X5
0.0X0
Time
121
-------
r±le,S975809 f 1-430 AcqtlO-SEP-1997 21:48:09 EI+ Voltage SIS 70S Noise: 809
407.7818 Ti4 BSU3(3S6,30,-3 .0 ) PKD(7r5,3,0.05\,3236.0,1.00\tF,T) XxpiXPCOS
TRIANGLE LABS Text:O-H33-l TLH43057 UKT. TIME - 21:50
1001
ao:
60:
40:
20.
A3.B9X5
\
\
f\/ \ A6.01E4 AS. 98X4
1 \ /\ A Al 29X4 A6.41X3 Av A2.17E4
31:12 3l't24 31\36 31:48 32:00 32,12 32\24 32:36 32:48
.7.2X4
.5.7X4
.4.3X4
.2.9X4
.1.4X4
.O.OEO
Tim*
Flle:S975809 01-430 Acq: 10 -SEP -19 97 21>48:09 EH- Voltage SIS 70S Noise: 36
409.7789 r>4 BSUB(256,30,-3.0) PXD(7,5,3,0.05\,144.0,1.00\,F,T) XxptXPCOS
TRIANGLE LABS Text:O-K23-l TLH43057 UKT. TDfX - 21:50
1001
80:
60:
40:
20:
Al . 6SE5
h
i
/ \ A4.91E4 AS. 95X4
/ \ A A_ A /v «•««
f^J \^_^^ /•* \->__/ V ^ ^ *. n <~ rr *• *• —^-/ ^^_ >V/V ^^ ^~S*^^ ^^_
31:12 31\24 31:36 31*: 4 8 32iOO 32:13 32\24 32i36 32\48
.5. 0X4
.4.0X4
.3.0X4
.2. 0X4
J9.9X3
0.0X0
Time
Tile:S975809 il-430 AoyilO-SXP-1997 21:48:09 XI+ Voltage SIS 70S Noise: 4 23
417.8253 T:4 BSOS(356, 30, -3.0) PXD(7,5,3,Q.05\,1692.0,1.00\,F,T) XxptXPCOS
TRIANGLE LABS Tazt:O-M23-l TLH43057 UKT. TIME - 21t50
1001
ao:
60:
40:
20:
A3.66E6
A
/ \ A2.41E6
II A
A
\ \
7 v_ / V
.1.3X6
'-.1.1E6
-.8.0X5
.5.3X5
.2. 7X5
O.OEO
3l',12 31:24 31:36 31:48 32iOO 32': 12 32\24 32': 36 32:48 Time
rlla:S97S809 tl-430 AcqtlO-SEP-1997 21:48:09 EH- Voltage SIS 70S Noiae:4S5
419.8330 tt4 BSOB(356,30,-3.0) PXD(7,S,3,O.OS\,1940.0,1.00\,r,T) ExptEPCOS
TRIANGLE LABS Tttxt:0-M23-l TLH43057 XKJ. TIME - 21:50
1001
80:
60:
40:
20:
A8.29E6
A
/ I AS. 76X6
A
A
y I y v
-2.9X6
.2.3X6
.1 . 8E6
.1.2X6
.5.8X5
' 0 . OEO
' 3l'tl3' ' ' 31\34~ ' '31:36 31:48 33,00 32:12 32t24 32\36 33\48 Tiae
Tile:S975809 tl-430 Acq:10-SEP-1997 21:48:09 EH- Voltaye SIS 70S
430.9739 F:4 EzptXPCUS
TSIANSLE LABS TejfttO-M23-l TLH430S7 UTJ. TIME - 21s50
1001
aol
60.
40.
20.
0
31:39 31:37 31:53 32:07~^33*\jL~~*~J3i32-*. ^~^r^}^?—*~'
^ — ^^~^~J~vv*-^^s~^^ ^/
2.2X6
.1.8X6
.1 . 3X6
.9 . 0X5
.4.5X5
0.0X0
' 31:12' ' ' 31\24~ ' ' 31\36 ' 31i48 32tOO 33il3 32\24 32s36 32:48 Time
rile:S975B09 fl-430 Aoq:10-SXP-1997 21:48:09 EH- Voltage SIS 70S
479.7165 F:4 XzptXPCOS
TRIANGLE LABS Text:O-M23-l TLH43057 IK7. TIME - 21:50
1001
80.
60.
40.
20.
0.
33,19
I 32,35
31,31 A , |
3ii°7 A hi ";" N A
^ Ajuw«^x ^^A A JLM i^M
A/ Lw L^v v 'V\^ii^A_jS/\_-Ay v i VNA^v V V_J L_yv \_^\J \_AJ k; VvA/* ^J
' 3l'tl2' ' ' 3l':24' ' ' 3l's36' ' '31:48 32:00 32:12 32:24 32:36 32\48
-8.6X3
.6.9X3
.5.1X3
.3.4X3
.1.7X3
0.0X0
Time
00
-------
nj.»tSS75B09 tl-430 AcqtJ.0-SEf-J.yS7 ill4»,O9 fH+ VOJ.t*g* SIX TOO JK>lt»,J7
423.7766 f,4 BSOB(256,30,-3.0) PXD(7,5,3,0 .OS\,14».0,1.00\,r,T) Xxp, SPOTS
TRIANGLE LABS Tmxt,O-H23-l TLI443057 JOKT. TIMS - 21t50
1003k A9.90X4
m*iS975809 tl-430 AcqtlO-SXP-1997 21,48,09 EI+ Voltage SIX 70S Koi»»,33
425.7737 Fi4 BSOt(256,30,-3.0) PXS(7, 5, 3,0. 051,132. 0,1.00\,r,T) XxpiXPCUS
TRIANGLE LABS T*xt,O-M23-l TLIt430S7 OKT. TIMS • 21,50
1001 A1.00JE5
A7. 72E4
-3.1E4
A9.27X3 I U AS.87X3
.0.010
31; 18 31,24 31:30 3l',36 31,42 3l',48 31,54 32,00 32', 06 32,12 32,18 32,24 32,30 T±mu
3.9X4
A7.47E3
31,18 31', 34 31,30 31,36 31,42 31,48 31,54 32,00 32,06 32,12 32,18 32,24 32,30
rilm,S97S809 tl-430 Acq,10-SEP-1997 21,48,09 EH- Voltage SIX 70S NoiM9,1060
435.8169 r,4 BSUB(256,30, -3.0) PO>(7, 5,3,0.05\,4240.0,1.00\,r,X) XxpiXPCUS
TRIANGLE LABS T*xt,O-M23-l TLH43057 UKT. TOOt - 31*50
1001
801
601
401
201
A6.70I6
o.oro
Tim*
-3.3X6
.1.9X6
.1. 4X6
19.3X5
.4.6X5
31,18 31,24 31,30 31,36 ' '31:42 ' '31,48 ' '31,54 ' '32,00 32,06 32,12 32,18 32,24
r±le,S975809 tl-430 Acq:10-SEP-lS97 21,48,09 EH- Voltage SIX 70S Bb±f»,530
437.8140 r,4 BSOB(256,30,-3.0) PKD(7,5,3,0,05\,2120.0,1.00*,r,T) XxpiXPCOS
TRIANGLE LABS T*Xt,0-M23-l TLI#43057 ZK7. TBCC " 21,50
1001 A6.J7E6
801
601
401
20.
. oxo
Tim*
01
^2.2X6
.1.8X6
.1.3X6
.9.0X5
.4.5X5
31,18 31,24 31,30 31,36 31,42 31,48 31:54 32,00 32,06 32,12 32118 32,24 32,30
Fil»iS975a09 tl-430 Acy,10-SXP-1997 21,48,09 EH- Voltagr* SIS 70S
430.9729 T:4 SxpiXPCUS
TKIANGLE LABS T«xt:O-M23-l TLIt43057 ItU. TZMT • 21,50
0.0X0
ttmm
1003
80.
60.
401
201
01
31,23 31,29
31,37
31t46^ 31,52
32*16
32129
31,18 31,24 31,30 31,36 31,42 31,48 31:54 32,00 32,06 ' '32,12 ' '32118 ' '32\24 ' 32,30
.2.2X6
.1.8X6
.1.3X6
.a.oxs
.4.5X5
0.0X0
Zinc
'•J.
123
-------
F±1»:S975809 tl-430 Aoq,10-SXP-1997 21,48,09 EI+ VoltMgm SIX 70S Hoia»,34
441.7428 r,4 BSOB(256, 30, -3.0) PKD(7 ,5,3,0. OS\,136 .0,1. 00\,r,T) XxptXPCOS
TKIANGLS LABS TfxtiO-H23-l TLH430S7 XKT. TIHX - ill 50
1003
901
aol
701
6ol
sol
401
301
20.
10.
A1.14E4
IA1.03X4
A6.63X3 A3.eix3 1 1
juAM . » Jl AM. _Avjft/uivA\M Ajiflx.
-2.4X4
A4.41X4
1 A1.01I4
*<>07X3 \ 33X3 1
JvvUxl^wA/ Uju\AJU-jivu^\LJlAJl
.2.2X4
.1.9X4
.1 . 7X4
.1.5X4
.1.2X4
.9.7X3
.7.3X3
.4.9X3
.2.4X3
O.OfO
Jit 00 32,00 33,00 34,00 35,00 X±m*
Fil«iS975809 tl-430 Acq,10-SEP-1997 21,48,09 EH- VoltMgm SIX 70S Hoim»,27
443.7399 T,4 BSOB(256, 30, -3.0) PXD(7,5, 3, 0. 05\,108.0, 1.00\,T,T) XzptEPCUS
TRIANGLE LABS T*xt:0-H23-l TLH43057 HKT. TIMX - 21,50
1001
901
801
701
601
501
401
301
201
101
A8.89E3
A8.12X3 1 A5.60E3
AS. 88X3 1 1 1
I I A3 . 75X3 I 1 A4 . 4
_1 . 6X4
AS. 93X4
1
1 A1.75W
1
1
'
. I A7.47E3
1 1
n 1
1 \A5.98E3 .1 A3.42X3^'i A4.48l| *6.56X3\ **'? >A3.98K3\ I . Ik 1 .
^WwJ^MVh^^ \MWvJlAJ\>AvAAA
.1.5X4
.1.3X4
.1.1X4
.9.8X3
.8.2X3
.6.6X3
.4.9X3
13.3X3
Ll . 6X3
'• 0 . 0X0
'jltOO 32,00 33\00' ' ' 34,00 ' 35,00' ' ' ' ttmm
ril»,S975809 tl-430 AoqilO-SXP-1997 21,48,09 EI+ Voltagw SIX 70S
430.9739 F,4 ExpiEPCUS
TRIANGLE LABS T*JCtsO-H23-l TLIt43057 UKT. TIMX - 21s 50
1004
901
aol
701
601
501
401
301
201
101
0
32,16 33,04 33,44
\ l1*"3 ^AlMAAAif3 M/^W^VlujU/WA AA^WVU.
\/^A/V\/w/VT'^Y>V v^"^ WUT ^
V
Jl:00 32\00 33\00
IA JIT 34,3434,52 35,36 2.4X6
.if . 1 4.A.* . MA.XN \ »1 /Afc
Mr/S^^Hfm^^
J "if
.2.2X6
.1.9X6
.1 . 7X6
.1.4X6
.1.2X6
.9 . 6X5
.7.2X5
.4 . 8X5
.2.4X5
'• 0 . 0X0
3uJ^^
.1.4X4
.1.2X4
.1.1X4
.9.2X3
.7.7X3
.6.2X3
.4 . 6X3
.3.1X3
.1.5X3
0.0X0
J4»00 ' J5iOO Tim*
124
-------
Fil»lS9758O9 ti-tJO AogtlO-SKf-lilil/ 21:4B:09 EI+ VOlt*g* SIX 708
457.7377 r:4 BSVB(256,30,-3.0) PXD(7,5,3,0.05\,112.0,1.00\,r,T) ExpiXPCOS
TRIANGLE LABS Taxt,O-M23-l TLIt43057 IKT. TIHX * 21:50
1004 A4.12E5
BO.
SO.
40.
20.
34154
34t24 34:30 34:36 34:42 34:48
Til*iS975309 fl-430 AogtlO-SEP-1997 21:48:09 EH- Voltage SIS 70S Jfoif»i34
459.7348 Tt4 BSUB(256,30,-3.0) fXD(7,5,3, 0.05%, 136. 0,1. 00\,r,T) ExptETCOS
TRIANGLE LABS Tait:O-M23-l TLH43057 ISJ. TIMS - 211 SO
100* A4.5.2X5
80.
eo:
40.
20:
34:54
34:24 34:30 34:36 34:42 34:48
Til»tS975809 fl-430 AcqtlO-SXP-1997 21:48,09 EH- Voltagm SIX 70S JK>immt284
469.7779 Ti4 BSVB(256,30, -3.0) PXD(7,5,3,0.05\,1136.0,1. 00\,T,T) XxptXPCUS
TXIANSLX LABS TarttO-K2J-l TLH43057 HUT. TIME - 21:50
1001,
34,24 34,30 34,36 34',42 34',48 34,54
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-------
TLI Project: 43057
Client Sample: O-M23-1
Method 23 TCDD/TCDF Analysis (DB-225)
Analysis File: X973083
Client Project
Sample Matrix:
TLI ED:
Sample Size:
Dry Weight
GC Column:
Azr##L.T ViAurr "A"
M23TRAIN
181-27-2A-C
1.000
n/a
DB-225
Date Received:
Date Extracted:
Date Analyzed:
Dilution Factor
Blank File:
Analyst
08/29/97
09/06/97
09/11/97
n/a
S975807
MS
Spike File:
ICal:
ConCat
% Moisture:
% Lipid:
% Solids:
SPC2NF04
XF24087
X973069
n/a
n/a
n/a
2,3,7,8-TCDF
EMPC
0.008
B
13C12-2,3,7,8-TCDF
2.4
59.8
40%-130%
0.79 22:31
p-..y; \f .*. •. > *ii^. ^s-tfO^^v 5'
!: Recovery Standard
t^> /xTJ..._^%^>_y...^
0.79 21:30
Data Reviewer
09/12/97
Page 1 of 1
ONFJ"S« «2jOOl LAIS &KL04
Triangle Laboratories, Inc.®
301 Capitola Drive • Durham, North Carolina 27713
3hone: (919) 544-5729 • Fax: (919) 544-5491
Printed: 14:59 09/12/97
131
-------
Initial
Date...
Data Review By:
Calculated Noise Area: n/a
The Total Area for each peak with an ion abundance ratio outside
ratio limit* has been recalculated according to method requirements.
Page No.
09/13/97
Listing of X973083B.dbf
Matched GC Peaks / Ratio / Ret. Time
Compound/
M_Z QC.Log Omit Why ..RT. OK Ratio Total.Area.. . Area.Peak.1.. Area.Peak.2.. Rel.RT Compound. Name.. ID..
Flag*.
TCDF
304-306 DC ML 0
18
19
:00
:42
:07
19:56
20
20
20
20
20
20
21
21
22
22
M 22
22
22
23
23
DC SN 23
23
23
DC SN 23
23
DC SN 24
24
24
24
DC WH 24
:00
:11
:15
:2S
:33
:46
:13
:29
:02
:24
:32
:49
:55
-.00
:08
:22
:28
:31
:37
:S4
:09
:27
:37
:39
:49
0.
RO
RO
RO
RO
RO
RO
RO
RO
RO
RO
RO
RO
RO
RO
RO
RO
RO
RO
RO
RO
RO
RO
RO
RO
65-0.89
1
1
0
1
1
0
0
0
0
0
0
2
0
0
1
2
0
1
2
0
1
0
0
0
4
0
1
1
0
.02
.65
.75
.59
.43
.71
.75
.15
.42
.58
.93
.97
.48
.38
.02
.09
.72
.70
.59
.17
.82
.75
.33
.23
.28
.29
.41
.31
.48
304-306 24 Peaks
13C12-TCDF
316-318 DC ML 0
DC WL 20
DC WL 20
DC WL 21
DC WL 21
22
22
23
DC WH 23
DC WH 23
DC WH 24
:00
:20
:43
:12
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:31
:42
:09
:43
:53
:30
0.
RO
RO
RO
RO
RO
RO
RO
RO
65
1
0
3
1
0
0
1
1
2
1
0
-0.89
.70
.71
.54
.10
.19
.79
.53
.19
.66
.02
.86
7.
8.
81.
7.
5.
14.
22.
3.
4.
88
25
84
31
31
69
SO
31
37
16.67
36.
4.
7.
7.
43.
4.
9.
a.
8.
2.
3.
11.
0.
5.
1.
6.
12.
9.
5.
341.
16
12
49
93
37
46
03
07
90
64
54
08
87
45
13
05
32
56
20
78
7
35
6
4
6
9
1
1
7
19
6
3
3
25
5
3
7
13
3
4
2
2
9
7
.68
.02
.57
.29
.11
.63
.44
.90
.25
.07
.93
.26
.45
.10
.27
.77
.76
.05
.63
.74
.37
.63
.82
.09
4.
46.
4.
3.
8.
12.
9.
4.
12.
20.
2.
6.
9.
24.
2.
5.
4.
5.
0.797-1.100
66
82
13
00
58
87
61
51
50
43
33
82
14
50
52
26
56
03
2.00
6.
10.
8.
6.
5.
34
22
94
96
40
0.000
0.830
0.849
0.885
0.888
0.896
0.899
0.907
0.913
0.922
0.942
0.954
0.979
0.995
1.001 2378 -TCDF AM
1.013
1.018
1.021
1.027
1.038
1.042
1.044
1.049
1.061
1.073
1.086
1.093
1.095
1.102
0.955-1.045
10.
11.
7.
92.
11.
21,370.
18.
62.
20.
10.
469.
34
53
50
73
36
95
07
41
90
87
56
9,401
15
42
.85
.64
.12
11,969.
10.
35.
10
21
26
0.000
0.903
0.920
0.942
0.954
1.000 13C12-2378-TCDF ISO
1.008
1.028
1.053
1.061
1.088
Triangle Laboratories, Inc.® Analytical Services Division
801 Capitola Drive • Durham, North Carolina 27713
Phone: (919) 544-5729 • Fax: (919) 544-5491
Printed: 14:59 09/1 2/97
132
-------
Page No. 2 Listing of x973083B.dbf
09/12/97 Matched GC Peak* / Ratio / Ret. Tine
Compound/
M_Z.... QC.Log Omit Why ..RT. OK Ratio Total.Area... Area.Peak.1.. Area.Peak.2.. Rel.RI Compound.Name.. ID.. Flags.
316-318 3 Peaks 21,451.43
Above: TCDF / TCDD Follows
13C12-TCDD 0.65-0.89 0.906-1.094
332-334 DC NL 0:00 0.80 63.88 0.000
20:08 RO 0.96 75.01 40.76 42.38 0.947
21:15 0.79 16,649.95 7,331.99 9,317.96 1.000 13C12-2378-TCDD IS1
21:30 0.79 25,684.70 11,297.00 14,387.70 1.012 13C12-1234-TCDD RSI
22:11 0.83 264.89 119.91 144.98 1.044
22:28 RO 0.22 22.00 9.57 42.82 1.057
22:40 RO 0.37 23.40 10.18 27.77 1.067
DC WH 23:49 RO 0.31 62.55 1.121
332-334 6 Peaks 42,719.95
Column Description 'why* Code Description QC Log Desc.
M_Z -Nominal Ion Mass(es) WL-Below Retention Time Window A-Peak Added
..RT. -Retention Time (mm:ss) WH-Above Retention Time Window K-Peak Kept
Rat.l -Ratio of M/M+2 Ions SK-Below Signal to Noise Level D-Peak Deleted
OK -RO-Ratio Outside Limits
-------
iJLfiX973O83 11-1285 Aog:li-SSP-19S7 22:34:33 00 20t00 21iOO 22:00 23:00 24:00
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136
-------
CO
Peak Locate Examination:ll-SEP-1997:22:34 File:X973083
Experiment:XCONF_TT Function:! Reference:PFK
Volts
-------
Pile;X9730B3 Jtl-1285 Acq;ll-gfiP-1997 22;34:29 GC EI+ Voltage 5IR AutoSpec
303.9016 Exp:XCONF_TT
Sample Text:O-M23-l TLI#43057 Pile Text: TRIANGLE LABS
lOOi A2.51E5
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60:
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20 j
Oj
21-iB'22:66'22-12'22:2*'22:36'22\iB'23\bb'23\12 23:24'23:36 23:48'24 166
File:X973083 #1-1285 Acq:ll-SEP-1997 22:34:29 GC EI+ Voltage SIR AutoSpec
305.8987 Exp:XCONF_TT
Sample Text:O-M23-l TLI#43057 File Text: TRIANGLE LABS
100%. A2.45E5
80J
60J
40:
20j
9.4E4
_7.5E4
_5.6E4
_3.7E4
_1.9E4
O.OEO
24:12 24:24
Time
OJ
21:48 22:00 22:12 22:24 22:36 22:48 23:00 23:12 23:24 23:36 23:48 24:00
File:X973083 #1-1285 Acq:ll-SEP-1997 22:34:29 GC EI+ Voltage SIR AutoSpec
315.9419 Exp:XCONF_TT
Sample Text:O-M23-l TLI#43057 File Text: TRIANGLE LABS
100*. 22JL31
801
60j
40J
20 j
OJ
9.0E4
L7.2E4
L5.4E4
L3.6E4
_1.8E4
O.OEO
24:12 24:24
Time
T i f i i
i i i i i i i i i i i i i r i i i i i i i i i i i i i i i i i i i i i i i i i i
21:48 22:00 22:12 22:24 22:36 22:48 23:00 23:12 23:24 23:36 23:48 24:00 24:12
i
2.1E7
L1.7E7
-1.3E7
_4.3E6
' ' I1'
24:24
O.OEO
OO
CO
Time
-------
TLI Project: 43057
Client Sample: O-M23-2
Method 23 PCDD/PCDF Analysis (a)
Analysis File: S975810
Client Project
Sample Matrix:
TLI ID:
Sample Size:
Dry Weight
GC Column:
2,3,7.8-TCDD
1,2^,7,8-PeCDD
1.23.4,7.8-HxCDD
!A3,6,7,8-HxCDD
1,2^,7,8.9-HxCDD
1.23,4.6,7,8-HpCDD
1.2,3,4,6,7,8,9-OCDD
M23TRAIN
181-27-3A-C
1.000
n/a
DB-5
: ^^*?i#
"A"
ND
ND
ND
EMPC
ND
EMPC
0.19
Date Received:
Date Extracted:
Date Analyzed:
Dilution Factor
Blank File:
Analyst
*r-: ;^:v
0.006
0.008
0.01
0.01
08/29/97
09/06/97
09/10/97
n/a
S975807
ML
;
0.02
0.04
Spike File:
ICal:
ConCal:
% Moisture:
%Lipid:
% Solids:
0.90
SPX2
SF56!
S97K
n/a
n/a
n/a
34:34
3704
L17
797
—
-
^^^~
B_
2^,7,8-TCDF
1,2,3,7,8-PeCDF
2^,4,7,8-PeCDF
1,2^,4,7,8-HxCDF
1,2^,6,7,8-HxCDF
2^,4,6,7,8-HxCDF
1,2^,7.8.9-HxCDF
1,2^,4,6,7,8-HpCDF
1,23.4,7.8,9-HpCDF
1,2^,4,6,7,8,9-OCDF
0.03
ND
ND
0.04
0.01
0.02
ND
0.07
0.02
0.06
0.006
0.006
0.008
0.79
1.27
1.21
1.37
0.88
1.19
0.95
20:27
28:25
28:32
29:02
31:14
32:25
34:42
B_
B_
B_
PRB
PRB
B_
B_
Total TCDD
Total PeCDD
Total HxCDD
Total HpCDD
Total TCDF
Total PeCDF
Total HxCDF
Total HpCDF
0.02
0.03
0.08
0.04
0.04
ND
0.11
0.12
5
3
0.06
0.10
0.08
0.006
Triangle Laboratories, Inc.*
801 Capitola Drive • Durham, North Carolina 27713
Phcroe: (919) 544-5729 - Fax: (919) 544-5491
Page 1 of 2
xrnjw vzot. LABS 6.100*
^^•••^•••^^^^••••B
Printed: 14:57 09/11/97
139
-------
TLI Project 43057
Client Sample: O-M23-2
Method 23 PCDD/PCDF Analysis (a)
Analysis File: S975810
I3C,r2,3,7.8-TCDF
'3Cl2-lA3
13Cn-lA3
13Ci2-l,2,3
13C,2-l,2,3
15Cu-l,2,3
l3C«-l,2,3
l3Cu-lA3
.7.8-PeCDF
.7,8-PeCDD
,6,7,8-HxCDF
,6,7,8-HxCDD
4,6,7,8-HpCDF
,4,6,7,8-HpCDD
,4,6,7,8,9-OCDD
2.2
23
2.4
2.6
2.4
1.7
1.8
2.2
6Z4
55.6
57.6
60.5
65.7
58.8
41.3
44.9
27.5
40%-130%
40%-130%
40%-130%
40%-130%
40%-130%
40%-130%
25%-130%
25%-130%
25%-130%
0.75
0.81
1.45
1.55
0.50
1.24
0.44
1.05
0.86
20:26
21:16
24:45
25:54
28:31
29:14
31:13
32:04
34:34
13Co-2,3,4,7,8-PeCDF
l3C,rl,2^,4,7,8-HxCDF
13Cu-lA3,4,7,8-HxCDD
13Co-lA3,4,7,8,9-HpCDF
4.0
3.4
3.7
3.7
3.4
98.8
85.1
92.1
91.9
84.9
70%-140%
70%-140%
70%-140%
70%-140%
709fe-140%
1.43
0^0
1.23
0.42
21:17
25:33
28:24
29:09
32:25
nate Standards (Type A) Ami. (ng)
--- ^."^jfj^^ssfy*. -"!-.-^NV .<^ .....^f
l3C,j-lA3.7,8,9-HxCDF
l3Cir2,3.4.6,7,8-HxCDF
2.2
2.5
54.3
62.0
40%-130%
OJO
0.49
29:44
29:01
BoweryStawianisf'V //:<^t> %i~w >
13C,2-U,3.7.8,9-HxCDD
0.82
1.22
21:02
29:31
Data Reviewer
09/11/97
Page 2 of 2
XZ37JM TUB, UUU &1OM
Triangle Laboratories, Inc.®
801 Capitola Drive • Durham, North Carolina 27713
Phone: (919) 544-5729 • Fax: (919) 544-5491
Printed: 14:57 09/11797
140
-------
)ata Review By:
Calculated Noise Area:
1.67
The Total Area for each peak with an ion abundance ratio outride
ratio limits has been recalculated according to method requirements.
Page No.
09/11/97
Listing of S975810B.dbf
Matched GC Peaks / Ratio / Ret. Tiae
Compound/
H_Z QC. Log Omit Why ..RT. OK Ratio Total. Area. .. Area. Peak. 1. . Area. Peak. 2.. Rel.RT Compound. Hue.. ID.. Flag*.
rcDF
304-306
304-306
D
D
D
D
D
D
D
D
D
A
D
DC
D
D
D
D
D
D
D
D
D
D
DC
NL
SN
SM
SN
SN
SN
SN
SN
SN
SN
SN
SM
2
0
16
17
17
18
18
18
19
19
19
19
20
20
22
:00
:59
:28
:43
:09
:31
:S6
:16
:36
:44
:58
:27
:57
:09
0.
RO
RO
RO
RO
RO
RO
RO
RO
RO
RO
65-0.89
0
1
0
0
0
1
1
0
0
0
0
0
0
1
.08
.01
.95
.64
.93
.05
.79
.77
.96
.68
.65
.79
.54
.26
Peaks
13C13-TCDF
316-318
316-318
TCDD
320-322
D
D
D
DC
DC
DC
DC
D
DC
DC
DC
D
DC
DC
DC
D
DC
DC
DC
DC
NL
WL
3
NL
WL
SN
SN
SN
SN
SN
SN
SN
SN
SN
SN
SN
SN
WH
0
19
19
20
20
:00
-.16
:57
:26
:56
0.
RO
RO
65
8
1
0
0
0
Peaks
0
18
18
18
19
19
19
20
20
20
20
21
21
21
22
22
:00
:10
:21
:50
:22
:23
-.42
:00
:14
:40
:51
:09
:21
:49
:10
:38
0.
RO
RO
RO
RO
RO
RO
RO
RO
RO
RO
RO
65
1
0
0
0
0
1
1
0
0
1
1
0
0
0
0
0
-0.89
.71
.10
.68
.75 3
.78
3
-0.89
.00
.57
.71
.67
.82
.41
.28
.98
.78
.32
.20
.93
.26
.30
.31
.85
0
5
4
8
10
7
4
11
16
11
16
31
4
1
48
0
5
23
,447
17
.14
.79
.05
.05
.80
.97
.09
.50
.41
.99
.82 6.62
.20 13.81
.94
.91
.02
.12
.22
.12 9.34
.55 1,477.22
.22 7.52
0.823-1.104
0.000
0.831
0.855
0.867
0.888
0.906
0.927
0.943
0.959
0.966
10.20 0.977
17.39 1.001 2378-TCDF AN
1.025
1.084
0.951-1.049
0.000
0.943
13.78 0.976
1,970.33 1.000 13C12-2378-TCDF ISO
9.70 1.024
,487.89
0
0
14
6
0
0
0
4
2
1
0
4
0
0
0
3
.14
.67
.55 6. OS
.41
.31
.60
.64
.64
.15
.61
.44
.71
•85
.46
.78
.31
0.857-1.061
0.000
0.854
8.50 0.863
0.886
0.911
0.911
0.926
0.940
0.951
0.972
0.980
0.995
1.004
1.026
1.042
1.064
Triangle Laboratories, Inc.® Analytical Services Division
301 Capitola Drive • Durham, North Carolina 27713
3hone: (919) 544-5729 • Fax: (919) 544-5491
Printed: 14:57 09/11/97
141
-------
Page Mo.
09/11/97
Lilting of S97581.OB.dbf
Matched GC Peaks / Ratio / Ret. Tiae
Compound/
M_Z QC.Log Omit Why ..RT. OK Ratio Total.Area... Area.Peak.1.. Area.Peak.2.. Rel.RT Compound.Name.. ID.. Flag*.
320-322
13C12-TCDD
332-334
332-334
PeCDF
340-342
D
D
0
340-342
13C12-PeCDF
352-354
1 Peak
14.55
352-354
DC
DC
DC
DC
DC
DC
DC
D
DC
DC
D
D
D
DC
D
DC
DC
DC
DC
DC
DC
DC
DC
NL
SM
SN
SN
4
NL
SN
4
NL
SN
SN
SN
SN
SN
SN
SN
SN
SN
SN
SN
0
NL
SN
SN
SN
SN
6
0:00
19:44
21:17
21:25
21:45
21:55
22:21
22:29
Peaks
0:
19:
21:
21:
21:
21:
00
56
02
16
29
38
0.
RO
RO
RO
2,
2,
0.
11.
069.
8.
3.
1.
1.
1.
093.
07
72 11.72
93 2,069.93
38 8.38
53 3.53
48
31
57
56
65-0.89
18
0
0
0
1
0
Peaks
0:
22:
22:
23:
23:
24:
24:
25:
25:
25:
26:
26:
00
40
46
43
51
10
45
04
34
42
34
39
1.
RO
RO
RO
BO
RO
RO
RO
.33
.90
.82 4,
.81 2,
.35
.87
6,
32-1.78
1
1
0
1
1
0
1
3
1
1
1
1
.14
.06
.45
.67
.58
.84
.55
.28
.38
.80
.60
.06
Peaks
0:
23:
24:
24:
24:
25:
25:
25:
25:
26:
26:
00
SO
23
45
55
04
33
50
55
31
39
1.
RO
RO
RO
RO
RO
0.
11.
190.
484.
3.
33.
11
93 6.08
27 1,890.11
18 1,109.29
54
89 15.79
0.906-
0.
0.
1.
1.
1.
1.
1.
1.
1.094
000
928
001 37C1-TCDD
007
023
031
051
057
StJHl
0.906-1.094
0.
6.74 0.
2,300.16 0.
1,374.89 1.
1.
18.10 1.
000
937
989 13C12- 1234 -TCDD
000 13C12-2378-TCDD
010
017
RSI
IS1
720.27
TCDD / PeCDF Follovs --
0.
8.
1.
3.
14.
3.
6,
4.
11.
4.
4.
2.
0.
13
29
09
15
48
52
96
23
74
31
24
75
00
32-1.78
1
1
1
1
1
1
1
1
1
2
1
Peaks
.14
.25,
.34
.45 2,
.61
.14
.43 2,
.37
.50
.54
.00
5,
0.
7.
11.
733.
11.
14.
257.
3.
3.
4.
1.
036.
13
65 4.65
91 6.83
22 1,617.73
42 7.04
89 9.05
14 1,330.15
01
03
62
51
23
0.909-1.079
0.
0.
0.
0.
0.
0.
1.
1.
1.
1.
1.
1.
000
916
920
958
964
976
000 12378- PeCDF
013
033 23478-PeCDF
038
073
077
AN
AN
0.838-1.162
0.
3.73 0.
5.08 0.
1,115.49 1.
4.38 1.
7.92 1.
926.99 1.
1.
1.
1.
1.
000
963
985
000 13C12-PeCDF 123
007
013
032 13C12- PeCDF 234
044
047
071
077
IS2
SOR2
Triangle Laboratories, Inc.® Analytical Services Division
801 Capitola Drive • Durham, North Carolina 27713
Phone: (919) 544-5729 • Fax: (919) 544-5491
Printed: 14:57 09/11/97
- 142
-------
.ge No.
1/11/97
Listing of s975810B.dbf
Matched GC Peaks / Ratio / Ret. Tine
impound/
_Z QC.Log Omit Why ..RT. OK Ratio Total.Area... Area.Peak.1.. Area.Peak.1.. Rel.RT Compound.Name.. ID.. Flags
sCDD
56-358
A
D
56-358
3C12-PeCDD
68-370
168-370
IxCDF
J74-376
M
M
D
M
D
DC
DC
DC
DC
D
DC
DC
DC
DC
DC
DC
DC
DC
DC
D
DC
D
DC
DC
DC
NL
SN
SN
SN
SN
SN
SN
SN
WH
1
NL
SN
SN
2
NL
SN
SN
SN
SN
SN
SN
WH
0:00
24:00
24:18
24:30
24:47
24:57
25:06
25:19
25:56
26:24
26:46
Peaks
0:00
24:46
25:54
26:03
26:25
Peaks
0:00
27:25
27:34
28:25
28:32
28:39
28:50
29:02
29:12
29:48
29:53
30:00
30:15
1.
RO
RO
RO
RO
RO
RO
RO
RO
RO
RO
1.
RO
RO
1.
RO
RO
RO
RO
---- Acove: feciJF / Fetaju FOJ.JL.OWS ---
32-1.78
0
0
0
2
1
0
1
0
1
1
1
.71
.72
.44
.24
.32
.51
.06
.61
.87
.02
.12
0
14
1
1
14
1
5
1
2
2
2
28
.08
.08 8.56
.43
.94
.76 8.40
.56
.71
.32
.70
.12
.47
.84
32-1.78
1
1
1
1
1
.00
.53
.55
.38
.23
05-1.43
1
1
1
1
1
1
0
1
3
0
1
0
1
.19
.16
.25
.27
.21
.18
.72
.37
.08
.83
.16
.53
.09
0
3
1,606
161
3
.12
.04
.95 978.75
.72 93.83
.49
0.921-1.026
0.
11.90 0.
0.
0.
6.36 0.
0.
0.
0.
1.
1.
1.
000
927
938
946
957
963
969
977
001 12378-PeCDD
019
033
AN
0.845-1.155
0.
0.
630.20 1.
67.89 1.
1.
000
956
000 13C12-PeCDD 123
006
020
1S3
1,770.67
4
7
16
20
9
4
4
9
0
4
1
2
3
.49
.59 4.07
.00 8.88
.56 11.50
.40 5.14
.19
.81
.00 5.21
.85
.43
.97
.67
-47
0.957-1.053
0.
3.52 0.
7 . 12 0 .
9.06 0.
4.26 1.
1.
1.
3.79 1.
1.
1.
1.
1.
1.
000
961
967
996 123478-HxCDF
001 123678-HXCDF
005
Oil
018 234678-HxCDF
024
045 123789-HxCDF
048
052
061
AN
AN
AN
AN
374-376
PR
5 Peaks
62.55
13C12-HXCDF
384-386 DC
DC
DC
DC
DC
NL
SN
SN
SN
SN
0
28
28
28
28
28
29
29
30
:00
:11
:24
:31
:40
:43
:01
:44
:09
0.
RO
RO
RO
RO
RO
43-0.59
0
0
0
0
0
1
0
0
0
.89
.96
.50
.50
.28
.72
.49
.50
.70
1,
1,
1,
1,
3.
1.
591.
801.
4 .
1.
574.
197.
2.
17
43
97
94
35
75
02
58
31
0.859-1.141
0.000
532.51
600.54
519.44
400.47
1,059.46
1,201.40
1,054.58
797.11
988
.996 13C12-HXCDF 478 SDR3
.000 13C12-HXCDF 678 IS4
.005
.007
1.018 13C12-HZCDF 234 ALT2
1.043 13C12-HXCDF 789 ALT!
1.057
Triangle Laboratories, Inc.® Analytical Services Division
301 Capitola Drive • Durham, North Carolina 27713
Phone: (919) 544-5729 • Fax: (919) 544-5491
Printed: 14:57 09/11/97
143
-------
Page No.
09/11/97
Listing of S975810B.dbf
Matched GC Peaks / Ratio / Ret. Tiae
Compound/
M_Z.... QC.Log Omit Why ..RT. OK Ratio Total.Area,.. Area.Peak.1.. Area.Peak.2.. Rel.RT Compound.Name.. ID.. Flags.
384-386
4 Peaks
6,165.51
Above: HxCDF / HxCDD Follows
HxCDD
390-392
D
M
D
390-392
13C13-HXCDD
402-404
402-404
HpCDF
408-410
M
D
M
408-410
13C12- HpCDF
418-420
418-420
DC
DC
DC
DC
D
DC
DC
DC
DC
D
DC
DC
DC
DC
DC
D
DC
DC
DC
DC
DC
DC
NL
SN
SN
SN
SN
SN
SN
SN
SN
SN
WH
WH
2
NL
SN
4
NL
SN
SN
WH
WH
3
NL
SN
SN
2
0:00
27:57
28:11
28:16
28:25
28:39
28:47
28:53
29:00
29:09
29:14
29:32
29:42
29:50
Peaks
0:00
28:38
28:50
29:09
29:14
29:31
Peaks
0:00
31:14
31:26
31:34
32:25
32:34
32:39
32:52
Peaks
0:00
31:13
31:33
32:25
32:51
Peaks
1.
RO
RO
RO
RO
RO
RO
RO
RO
RO
1.
RO
RO
0.
RO
RO
0.
RO
RO
RO
05
1
1
4
0
1
1
1
1
1
1
0
0
3
0
-1.43
.63
.57
.05
.85
.23
.34
.02
.17
.37
.33
.95
.71
.86
.74
1.
4.
0.
0.
29.
10.
2.
0.
2.
4.
6.
5.
1.
1.
36.
50
03
43
63
72 16.41
90
11
91
58
06
41 3.55
35
25
86
13
05-1.43
0
1
0
1
1
1
.88
.13
.66
.23
.24
.22
1.
7.
1.
1,191.
1,332.
2,276.
4,808.
t*_4WM*
88-1.20
1
0
1
1
1
1
0
1
37
0
0
1
0
1
.55
.88
.03
.11
.19
.48
.96
.15
-0.51
.91
.44
.60
.42
.33
1.
22.
8.
6.
4.
1.
1.
4.
35.
1.
834.
1.
546.
26
89 4 . 18
77
87 657.77
37 737.61
32 1,249.58
45
90
50 10.50
11 4 . 11
87
98 2.71
57
92
22
59
47
38 254.39
17
46 161.53
0.
13.31
3.72
0.
3.71
534 . 10
594.76
1,026.74
0.
12.00
4.00
2.27
0.
579.99
384.93
1.40
1,380.
84
951-1.015
0.000
0.956
0.964
0.967
0.972
0.980
0.985
0.988
0.992
0.997 123478-RxCDD
1.000 123678-HxCDD
1.010 123789-HxCDD
1.016
1.021
966-1.034
0.000
0.979
0.986
0.997 13C12-HXCDD 478
1.000 13C12-HXCOD 678
1.010 13C12- HXCDD 789
995-1.045
0.000
1.001 1234678-HpCDF
1.007
1.011
1.038 1234789-HpCDF
1.043
1.046
1.053
936-1.128
0.000
1.000 13C12-HpCDF 678
1.011
1.038 13C12- HpCDF 789
1.052
AN
AN
AN
SOR4
IS5
RS2
AN
AN
IS6
SDR5
PR
Triangle Laboratories, inc.® Analytical Services Division
801 Capitals Drive • Durham, North Carolina 27713
Phone: (919) 544-5729 • Fax: (919) 544-5491
Printed: 14:57 09/11/97
144
-------
Page No.
09/11/97
Listing of S975810B.dbf
Matched GC Peak* / Ratio / Ret. Time
Compound/
M_Z QC.Log Omit Why ..RT. OK Ratio Total.Area... Area.Peak.1.. Area.Peak.2.. ReL.RT Compound.Name.. ID.. Flag*.
HpCDD
424-426
424-426
13C12-HpCDD
436-438
436-438
OCDF
442-444
442-444
OCDD
458-460
458-460
13C12-OCDD
470-472
470-472
DC
DC
DC
DC
DC
DC
DC
DC
DC
DC
DC
DC
DC
DC
DC
DC
DC
DC
DC
DC
DC
DC
DC
DC
DC
DC
DC
NL
SN
WH
WH
2
NL
SN
1
NL
SN
SN
SN
SN
SN
SN
SN
SN
SN
SN
SN
SN
SN
SN
SN
SN
1
NL
SN
1
NL
WH
1
0
31
31
32
32
32
:00
:29
:42
:05
:17
:29
0.
RO
RO
RO
RO
RO
- - - - Aoove : Hjx-ur
88-1.20
1.
1.
2.
0.
0.
0.
30
05
92
86
28
50
Peaks
0
31
32
-.00
:28
:04
0.
RO
1.
9.
0.
8.
0.
1.
17.
/ npuju toxiowa --•
16
61 4.92
75
12 4.14
65
20
73
88-1.20
1.
0.
1.
Peak
0
31
31
31
32
32
32
33
33
33
33
34
34
34
35
35
35
35
-.00
:26
:36
:56
:12
:22
:50
:17
-.24
:30
:43
:00
:29
:42
:01
:25
:34
:55
0.
RO
RO
RO
RO
RO
RO
RO
RO
RO
RO
RO
RO
RO
RO
RO
16
26
05
76-1.02
1.
0.
2.
2.
0.
0.
0.
0.
1.
0.
0.
6.
0.
0.
0.
1.
0.
1.
29
93
06
40
18
57
59
04
71
64
58
26
41
95
11
86
99
45
Peak
0
34
34
:00
:34
:58
0.
RO
RO
1.
1.
833.
38
04
58 427.57
833.58
HpCDD / Octa-CDD and CDF
0.
1.
0.
1.
0.
1.
0.
0.
1.
0.
0.
0.
0.
7.
0.
1.
2.
0.
7.
13
43
59
19
45
44
96
17
36
57
38
36
74
27 3.55
19
06
13
21
27
76-1.02
1.
0.
0.
17
90
16
Peak
0
34
35
:00
:34
:04
0.
RO
RO
76-
0.
0.
2.
1.02
67
86
39
Peak
0.
17.
0.
17.
0.
650.
1.
650.
11
03 8.09
30
03
08
55 301.53
74
55
0.977-1.006
0
4.69 0
0
4.83 1
1
1
.000
.982
.989
.001 1234678-HpCDD
.007
.013
AN
0.969-1.031
0
0
406.01 1
0.884
0
0
0
0
0
0
0
0
0
0
0
0
0
3.72 1
1
1
1
1
0.884
0
8.94 1
1
0.996
0
349.02 1
1
.000
.981
.000 13012-HpCDD 678
-1.116
.000
.909
.914
.924
.932
.936
.950
.963
.966
.969
.975
.984
.998
.004 OCDF
.013
.025
.029
.039
-1.116
.000
.000 OCDD
.012
-1.005
.000
.000 13C12-OCDD
.014
IS7
AN
AN
isa
Triangle Laboratories, Inc.® Analytical Services Division
801 Capitals Drive • Durham, North Carolina 27713
Phone: (919) 544-5729 • Fax: (919) 544-5491
Printed: 14:57 09/11/97
145
-------
Page Ho. 6 Listing of S975810B.dbf
09/11/97 Matched GC Peaks / Ratio / Ret. Time
Compound/
H_Z.... QC.Log Omit Why ..RT. OK Ratio Total.Area... Area.Peak.1. . Area.Peak.2.. Rel.RT Compound.Name.. ID.. Flags.
Column Description "Why" Code Description QC Log Desc.
M_Z -Nominal Ion Mass(ea) WL-Below Retention Time Window A-Peak Added
..RT. -Retention Time (mm:as) WH-Above Retention Time window K-Peak Kept
Rat.l -Ratio of M/M+2 Ions SN-Below Signal to Noise Level D-Peak Deleted
OK -RO-Ratio Outside Limits
-------
Tile * 59 75810 #1-848 AcqtlO-SEP-1997 22*27:32 EH- Voltage SIS 70S Noi*mi28
303.9016 Tt2 BSOB(256, 30, -3.0) PXD(9,5,5,0.051,113.0,1.00\,r,T) Exp:EPCOS
TRIANGLE LABS T»xt:O-H33-2 TLH43057 XK7. TIME - 22*30
1004 A1.38X5
17:00 18*00 19*00 20*00 21*00
rile*5975810 #1-848 Acq:10-SEP-1997 22t27:32 EH- Voltage SIS 70S Holt*:367
305.8987 1:2 BSUB(256,30,-3.0) PB>(9,5,5,0.05\r1468.0,1.00\,r,T) ExpiKPCOS
TRIANGLE LABS Texts0-M23-2 TLH43057 1X7. TIME - 22*JO
1001 A1.74X5
22iOO
17>00 18*00 1.9*00 20*00 21*00
rile:S975810 #1-848 Acq: 10-SEP-1997 22:27:32 EH- Voltage SIS 70S Noia»>304
315.9419 T>2 BSUB(2S6,30, -3.0) PKD(9,5,5 ,0.05\,1216.0,1.00\,r,T) XzptXtCOS
TRIANGLE LABS TexttO-M23-2 TLH43057 UfJ. TIME ' 32:30
100]
so:
so:
40:
20:
o:
22*00
17*00 18*00 19*00 20*00 21*00
M_le:S975810 #1-848 AcqslO-SEP-1997 22:27:32 SI+ Voltage SIS 70S Soim»:34
317.9389 1:2 BSUB(256,30,-3.0) PKD(9,5,5,0.05\,136.0,1.00\,r,T) ElpiEPCUS
TSIASGLE LABS Text:O-M23-3 TLH43057 IMT. TIMS " 33t30
1001 A1.97E7
80:
so:
40:
20:
o:
17:00 18*00 19*00 20(00
File:S975810 #1-848 Acq:10-SEP-1997 22:27:32 XI+ Voltage SIS 70S
330.9792 1:2 HrptEPCUS
TKJAKBIE LABS T«xt.-O-M2J-2 TEJ#43057 IJKT. TIME
100*
20:38
tO. 47
17,1. «.«
so:
21*00
17:00 18:00 19*00 20*00
rlle*5975810 #1-848 AcqilO-SEP-1997 22:27:32 EH- Voltage SIS 70S
375.8364 T:2 Xxp:XPCUS
TRIANGLE LABS T*xt:O-H23-2 TLIH3057 IJKT. TIME ~ 22:30
100\
17:51
22:00
I 18,23 19*18 ! I
jLlJUuii^^
17*00
18*00
19 00
20*00
.3.5E6
-2.8X6
.2.1X6
.1.4X5
-7.015
.0.020
Time
-4.8X6
.3.9E6
.0. OEO
Tim,
21*00
22*00
147
-------
.' ^
ttla:S975810 tl-848 AcfilO-SXP-1997 22:27:32 EI+ Voltage SIX 70S Ho±»9:38 ; « i£T
319.8965 T*2 BStn>(256, 30, -3.0) PKD(7, 5,3,0. 05\, 152. 0,1.00\,r,T) XxptXPOTS / \ l>
TRIANGLE LABS T»xt:0-H23-2 TLI443057 OU. 2XM9T • 22:30 ,. "
100]
80:
50:
"•THR
20:
0
A6.05E4 \.J 1.5X4
| A2.58X4 y •
A2.92E4 '••' 1A ^'^^
1 A A2.48S4 ^f.f
Jill «rf.7tf*J Jl J A7.97E3 ' i |
I'l' ftlWl A1'l°E4 ,*8.56X3 l^A9.40xI\ *3 ' ?4*? '1 IlL 3 . 73S3 1 A5.10*3 |ii
ixJ IwjiVvJ nAANV/uAAWwAN/Jr lu/V^A/v IA^ uv«lA/'U^ VAA/AA IL/iAJUlA/miLAA^^^iriL
isioo' ' \3oloO 21\OQ '22:00
.1.2C4
.8.9X3
.5 . 9X3
.3.0X3
0.0X0
Fll»:S97SaiO tl-848 Acq: 10 -SEP- 19 97 22:27:32 XH- VoltMy* SIX 70S Hoi**t38
321.8936 F:2 BSVB(256, 30,- 3.0) PKD(7,5,3,0.05\,152.0,1.00\fT,T) XxptXPCUS
TRIANGLE LABS Text:O-H23-2 TLH43057 OKT. TIKE - 22:30
1001
80:
50:
!. 10.
20:
A8.50E4
l\ A3. 20X4
M A3. 83X4 A2.62X4 1
I tt A4.38« |< 1 A9.UX3 ftl 45.55fJ AS. 77X3
l\ |H A*.?5«| ij.MB/l * 1 1 AAHb .7.M..I 1 .Alf??W
.*/* U .jV \^/U^AAJLJlU_A/V V A Jd\ J^A.^Art/^•^VMl/V^U^AJIAft« JWA, JUAIlU.M/m/
15:00 20:00 21*00 22:00
.1.8X4
.1.5X4
-L.1E4
.3.6X3
• o . oxo
Til»:S975810 tl-848 AcqtlO-SXP-1997 22:27:32 EH- Volt*y» SIX 70S Hoi**tS50
331.9368 T:2 BSVB(256, 30, -3.0) PXD( 7,5, 3,0 .05\,2200.0,1.00\,r,T) XzptXPCUS
TRIANGLE LABS Text.:O-H23-2 TLIt43057 OCT. TIME - 22:30
100]
80:
50J
40:
20:
0
A1.89E7
\
\\A1.11X7
ft
y V; \
15»00 ' 20»00 21:00 ' ' ' '22tOO
.4.8X6
-.3.8X6
.2.9X6
.1.9X6
.9.6X5
•o.oxo
TiMm
File :S975 810 tl-848 AcqilO-SXP-1997 22:27:32 SI+ Voltage SIX 70S SoiM»t28
333.9338 Fi2 BSVB(256,30,-3.0) PKD(7, 5,3,0. 05*,112. 0,1. 00*,f,T) Exp:EPCVS
TRIANGLE LABS T*Xt:0-M23-2 1X1*43057 HCT. OTKE • 22:30
ion
80:
601
40l
20:
o'-
A2.30E7
\
\rT7
ft
> \> \
19:00 20:00 21:00 22:00
3.8X6
.4.7X6
.3.5X6
-.2.3X6
.1.2X6
'• o.oxo
TlM*
F±lo:S975810 tl-848 AcqslO-SEP-1997 22:27:32 EH- Voltagmi SIX 70S Hoia»:3S
327.8847 Ts2 BSVB(2S6,30,-3.0) Pia3(7,5,3,0.05\,140.0,1.00\,r,X) ExpsEPCUS
TRIANGLE LABS Text>O-H23-2 TLIH30S7 X2K7. TUtE - 22:30
1001
80:
60:
401
201
0
A2.07E7
n
ft
7 V
19:00 20:00 21:00 '22:00
5.3X6
.4.2X6
.3.2X6
.2.1X6
.1.1X6
0.0X0
Timm
Fll»:S975810 tl-848 Aoq:10-SXP-1997 22i27t32 EH- Volttg* SIX 70S
330.9792 Tt2 Exp:EPCUS
TRIANGLE LABS T*xt.:0-H23-2 TU 44 3057 IKT. TIME " 22:30
100]
80.
60.
40.
20.
0
tt.Af 22*26 4.416
,„ „ 20:3820*56 ^ *1 >?l^ 2*,i*l~*J+^~^+~»*S+**
18,44 **i*I k ^J^y^^w>A<^^rn/Vv^Vx^r'wv^^-^^^^^^^
J£U? ,iS\ *19:OAv^-~*^*>^^WVkV^W^/
\X*^
v
' 19:00 20:00 21:00 22:00 '
,
.3.5X6
.3.6X6
.1 . 8X6
.8.8X5
0.0X0
T±mu
148
-------
riletS975810 #1-848 AoqilO-SXP-1997 22t27t32 EI+ Voltay* SIX 70S Hoim*:38
339.8597 Fs2 BSOB(256,30,-3.0) PKD(7,5,3,0.05%, 152.0,1.00\,rfT) SxptSPCUS
TRIANGLE LABS TttIt:O-M23-2 TLH43057 UKT. IZME "
A8.$6E4
A6.81X4
23100 24'tOO 25:00
TiletS975810 #1-848 AcqtlO-SXP-1997 22,27:32 XI+ Voltag* SIS 70S *oi»»:33
341.8557 Tt2 BSOB(256,30,-3.0) PXD(7,5,3,O.OS\,132.0,1.0Q\rr,T) XxptXfCUS
TRIANGLE LABS T*xt:O-M23-2 TLH43057 UKT. TOtX -
1QO\A4. 4E4
A6.01E4
AS.62X4
A8.26E3 W .J12.54E4
23:00 24i00 25:00
rile.S575810 #1-848 Acq:10-SEP-1997 22,27:32 EH- Volts ff» 5JZ 70S Xoim»:39
351.9000 r:2 BSUB(256,30,-3.0) PKX>(7,5,3,0.05\,156.0,1.00\rr,T) XxptEPCOS
TRIANGLE LABS T*xt:O-M23-2 TLIH3057 UKT. TIME -
A1.62E7
22:30
A4.23E4
A7.17E4 I 1 A5.44E4
22:30
26:00
22130
80:
60:
Oj
A1.33E7
OE6
0X6
OS6
0X6
0X6
0X0
26:00
23100 24:00 25:00
F±la:S975810 #1-848 Acq: 10-SEP-1997 22:27:32 EH- Volttym SIS 70S Voif»:37
353.8970 Ts2 BSUB(256,30,-3.0) PKD(7e5r3,0.05\,148.0,1.00\,r,T) EzptXPCOS
TRIANGLE LABS TtatsO-M23-2 TLH430S7 UKT. TIMS - 22:30
1004 A1.12E7
80:
6ol
40J
201
o:
A9.27E6
23:53 24i13
24:42
2J»00 24iOO .25(00
rile i SP 75810 #1-848 JlcgslO-SIP-1557 22:27:32 EI+ Voltage SIX 70S
330.9792 r:2 ExpiEPCVS
TRIANGLE LABS Taxt:O-K23-2 TLIt430S7 XK7.
JOOA 2Jf07 ,, , „,.„., 35s05
80J
so:
40:
201
o:
TIME -
25>33
26:00
22:30
25; 53
26:25 26:47
4.
.3.
.2.
.1.
.9.
rile »S5 75810 #1-848 Acq:10-SEP-1997 22:27:32 EI+ Voltmgm SI* 70S
409.7974 T:2 ExpiEPCUS
TRIANGLE LABS T*xtiO-M23-2 TLH43057 1X7.
TZMT -
26': 00
33130
4X6
7X6
0X6
3X6
7X5
0X0
Time
8X6
9X6
9X6
9X6
7X5
0X0
23100
24 100
23100
26:00
149
-------
"ilmiS97S810 tl-B48 AcqslO-SEP-1997 22:27:32 XI+ Valtmgm SIM 70S
355.8546 Tt2 BSUB(256,30, -3.0) ?KD(7,5,3,0.05\, 106.0,1.00\,r,T) XrptXfCOS
TRIANGLE LABS TOXt:O-N23-2 TLH43057 ZK7. TIKE - 22«30
1004 AS.40E4
24100 25100 26100
FilmtS975810 tl-848 AcqtlO-SEP-1997 22*27*32 EH- Voltag* SIS 70S JK>im»i3S
357.8516 Tt2 BSUS(256,30,-3.0) PXD(7,5,3,0.05\,140.0,1.00\,r,T) ExptEPCUS
TRIANGLE LASS TtattO-H23-2 TLH43057 IKT. TIME • 22.30
1001 A6.36E4
2.1X4
24:00 25t00 26:00
f±lmtS9"75810 tl-848 AcqilO-SEP-1997 22*27)32 EH- Voltfff» SIS 70S tfoimmi36
367.8949 Ti2 BSUS(256,30,-3.0) PKD(7,5,3,0.05\,144.0,1.00\,r,T) ExpiCPCUS
TRIANGLE LASS Text:0-M23-2 TLH43057 OU. TIHX " 22*30
1001 A9.79X6
80.
60.
40.
20.
).38E5
A
24>00 25>00 2fi»00
riletS975810 tl-848 AcqslO-SEP-1997 22t27i32 EI+ Voltage SIS 70S Hoim»t33
369.8919 T,2 SSUB(256, 30, -3.0) PKD(7,5,3, 0.051,132. 0,1.00\,r,T) ExpiXPCOS
TXIANGLX LASS TextiO-M23-2 TLH43057 1X7. TIKE - 22,30
1001 A6.30X6
80.
60.
40.
2QL
6.79S5
^
24:00 25:00 26tOO
fil»tS975810 tl-848 Aeq:10-SEP-1997 22:27:32 EH- Volttgu SIS 70S
330.9792 r*2 EzptEPCOS
TRIANGLE LABS T*It:O-M23-2 TLI443057 JK7. TIME - 22:30
1001
80.
60.
40.
20.
0.
3.6X6
2.9X6
.2.2X6
.1.4X6
.7.2X5
.0.0X0
Tim
.2.3X6
.1.9X6
.1.4X6
.9.3X5
.4.6X5
.0.0X0
Tim.
.4.8X6
'.3.9X6
'.2.9X6
.1.9X6
.9.7X5
0.0X0
24 tOO
25oO
150
-------
rile.-£975810 #1-405 Acq:10-SEP-1997 22:27:32 EI+ Voltage SIX 70S Jfc>i«e:1221
373.8208 ri3 BSV3(256,30,-3.0) PKD(7, 5,3, 0.05\,4884.0,1.00\,r,T) XxptXPCUS
TRIANGLE LABS Taxt:0-M23-2 TLH43057 HET. TXMK -
1001
27:24 27:35 27:48 28:00 28:12 28:24 28:35 28:48 29:00 29:12 29:24 29:36 29:48 30:00 30:12
rile:5975810 tl-405 Acq:10-SEP-1997 22:27:32 EH- Voltage SIX 70S Hoif»,1027
375.8178 F,3 BSU*(256,30,-3.0) PXDf 7,5,3,0.05%,4108.0,1.00%,JT,T> XxptXPCUS
TRIANGLE LABS Text:O-M23-2 1ZI#43057 XK7. TIME • 22:30
100^ A7.J.2E4 A9.38E4 _2
020
M*»
I
aW*
27,24 27:35 27:48
riles5975810 #1-405 Acq:JLO-SEP-1997 22:27:32 EH- Voltage SIX 70S Uoiam>935
383.8639 F,3 BSUt(256, 30, -3.0) PKD(7,5,3, 0.05\,3740.0,1.00\,TrT) XxptXPCOS
TRIANGLE LABS Text:O-M23-2 2ZJ#43057 JWT. TIME - 22:30
lOOi,
AS.19X6
80J
60J
40J
20:
ol
A4.00ES
27:24 27:35 27:48 28:00 28:12 28:24 28:35 28:48 29:00 29:12 29:24
rile:5975810 #1-405 Acq:10-SEP-1997 22:27:32 SI+ Voltage 5IX 705 Jfoi»«:1051
385.8510 f:3 BSOBC255,30,-3.0/ PKD(7,5,3, 0.051,4204.0,1.00\,r,X) XxptEPCUS
TRIANGLE LABS Text:O-M23-2 TLH43057 IJKT. TIME - 22:30
2.9:48 30i 30:12
100]
80:
so:
40:
20:
0.
A1.20E7
A1.0SX7
,
A7.97ES
J \
27:24 27:35 27:48 28:00 28:12 28:24 28:35 28:48 29:00 29:12 29:24 29:35'29:48 30:00 30:12
filejS975810 tl-405 AcqslO-SEP-1997 22:27:32 XI+ Voltage SIB 70S
392.9750 7:3 ExptEPCOS
TXIAHSLE LABS Tart:O-H23-2 JXJ#43057 ZKT. TtMT - 22:30
27:45 28:04 28:18 38!36 29l°J 29:20 29:37 - .. ^
100]
eo:
50:
40.
20:
o.
27:24
T
~r
?r
-r
, , , , - - i 11 i 11 11 111 11 i i 11 i 111 111111111 11111 111 1111111 111111111111 1111..
27:24 27:36 27,48 28,00 28:12 28:24 28:35 28:48 29:00 29:12 29:24 29:36 29:48 30:00 30:12
WlesSS75810 #1-405 Acq:10-SEP-1997 23,27,32 XI+ Voltage SIS 70S
445.7555 T,3 XfptEPCOS
TSIANGLX LABS T*xt:O-M23-2 1ZI#43057 JJKT. TIMS -
3X6
8X6
4X6
1X5
6X5
0X0
Tim*
6X6
7X6
.7X6
.8X6
.1X5
.020
Tin*
.4X6
.9X6
.4X6
.5X5
.8X5
.0X0
XlMJ
1001
ao:
50:
40:
20:
o.
27
28
Ms JO
29tl7
27i24 "27\36"27\48"2'a\ob' 28:12' 2B\24' 28^35 28:48' 29ioo'iiija'iilii'iiijj' 29»4i'
29:49 ;
-^AA^JwLuJiLJlAWA^jL i^0
i i i | i r < l i r l | i i i i i i i i' "
29:24 29:35 29:48 30:00 30:12
5ZJ
023
323
7X3
0X0
Tijtei
151
-------
'il.*:S37581Q ti-405 Acqt10-SEP-LS97 22>27s32 EI+ Voltage SIS 70S NOS.f*t545
89.8156 T:3 BSUB(256,30,-3.0) PKD(7,5,3,0.05\,2180.0,1.00\,T,T) SxptXPCUS
TRIANGLE LABS T*xtiO-M23-2 TLH43057 UKT. TIME » 22:30
1001 Al.l
80.
60.
40.
201
28:12 28:24
fll*:S975810 #1-405 AcqtlO-SXP-1997 22i27t32 EH- Volt*g* SIX 70S Hoia»:336
391.8127 Ti3 BSOB(256,30, -3.0) PO>(7,5,3, 0.OS\,1344.0,1.00\,T,T) EipiEPCUS
TRIANGLE LABS T*zt,0-M23-2 TLH43057 HKT. TIME - 22:30
1001 A1.33E5
27': 4 8 28:00 28:12 28:24 28:36 28i48 29:00 29:12 29t24 29:36 29:48
ril*iS975810 H-405 AcqtlO-SEP-1997 22:27:32 EI+ Volt*g* SIS 70S Kola*:348
401.8558 T:3 BSOS(256,30,-3.0) PKS(7,5,3,0.05\,1392.0,1.00\,r,T) XxpiXPCUS
TSIAKSLX LABS T*XtiO-M23-2 TUt43057 HKT. TIMX - 22,30
100.1 A1.25S7
A2.82E4
E
82X4
f\A7.
56t3
,^T^\^,^rf\T~r^TT'r^: i r^n
A6.25E4
A4.12E4
f^ f\r^r^~^i, i X^fT . i . i rY~T^? , . , r*|Qf^'T . ^V'TT?^' .O.OEO
28:36 28:48 29:00 29:12 29:24 29:36 29:48 Tim*
.6.3X4
.5.1X4
'.3.8X4
'.2.5X4
.1.3X4
.4.9X4
Tim*
80.
60.
40.
20.
A7.38E6
-5.0*5
14.015
.3.0X6
J.OX6
J.9X5
0.0X0
27:48 26:00 28:12 28:24 28:36 28:48 29:00 29:12 29:24 29:36 29:48
rll*:S975810 91-405 Acq:10-SEP-1997 22:27:32 EI+ Voltagu SIS 70S Kolt»i402
403.8529 f:3 3SOB( 256,30, -3.0) PJO3( 7,5,3, 0.05\,1608.0,1.00%, T, T) Erp:EPCUS
TSIANSLE LABS T*xt:O-M23-2 TLH43057 IOJ. TIME - 22:30
1004 A1.03E7
Tim*
80.
60.
40.
20:
0.
AS . 95 E6
-
27:48 28:00 28:12 28:24 28:36 28,48 29:00 29:12 29:24 29:36 29:48
ril*iS975810 #1-405 AcgtlO-SXP-1997 22:27:32 EI+ Volfeag* SIS 70S
.4.0X6
'.3.2X6
.2.4X6
.1.6X6
.8.0X5
0.0X0
Tim*
392.9760 ft3 ExpiXPCOS
TSIASGLE LABS T*xt:0-M23-2 TLH430S7
1001
IKT. TIME - 22:30
so:
50-
40:
20:
o:
v s^Swstfffi**~s*^^^ /^/VvwHV^v^^y-V
27\48 ' ' 28\00' ' '28:12 28:24 28\36 2a',48 29\6o 29': 12 29': 24 29': 36 29\4t
.2.3X6
Ll.srs
.1.415
^.1X5
14.5X5
10.0X0
M*
152
-------
File:SS75810 tl-430 AcqtlO-SEP-1997 22,27:32 EI+ Voltaffe SIS 70S Noi*»,719
407.7818 T,4 BSVB(256,30,-3.0) tXD(7,5,3,O.OS\,2876.0,1.00\,r,T) ExpiEPOJS
TRIANGLE LABS TmittO-H23-2 TLH43057 XK7. TIME - 22,30
1001 A1.55E5
80.
60.
40.
20^
A4.11E4
is
•*J.«CT
^
WV
-vVwyvv
J1J13 31', 24 31', 36 31:48 32,00 32*12 32*24 32*36
rile,3975810 tl-430 AcqilO-SEP-1997 22*27,32 EI+ Voltag» SIX 70S Noi*»,463
409.7789 r,4 BSUB(256,30,-3.0) PXD(7,5,3,0.05\,18S2.0,1.00*,r,T) ElpiXPCUS
TRIANGLE LABS TfXttO-M23-2 TLIt43057 UKT. TIME - 22,30
A1.33E5
32,48
80:
40J
"
A1.17X4
-A*
•.2.5E4
''.1. 7X4
-.8.3E3
77\
•^
31,12 31,24 31,36 31,48 32,00 32,12 32,24
rila,S975810 tl-430 AcqtlO-SEP-1997 22,27,32 XI+ Voltay* SIS 70S Koiu»:466
417.8253 F,4 BSUB(256,30,-3.0) PXJ>(7,5,3,0.051,1864.0,1.00\,r,T) ExptEFCUS
TRIANGLE LABS T*xt:O-M23-2 TLH43057 UZT. TIME - 22,30
1001 A2.S4E6
32,36
32,48
40
20:
OJ
A1.62E6
31,12 31,24 31s36 31:48 32,00 32:12 32,24 32*36
r±le,S975B10 tl-430 AcqtlO-SEP-1997 23s27t32 EI+ Volttgm SIS 70S Noll*,508
419.8220 F:4 BSOB(25S,30,-3.0) PKD(7,5,3,0.05\,3032.0,1,00\,r,T) SzptSTCOS
TRIANGLE LABS Tfxt,O-M33-2 TLIM3057 IKT. TIME - 22,30
1001 A5.SOE6
32:48
so:
so:
,S975810 tl-430 Acq,10-SEP-1997 22:27:32 EI+ Voltaye SIS 70S
430.9729 Ti4 ErpiEPCUS
TRIANGLE LABS TeitiO-H23-2 TLH43057 IXJ. TIME - 22:30
31>50 32tl3 32,30 32,38
32:48
1003
801
601
401
0:
.31,10
.31,2331^29
31:12 31,24 31,36 31,48 32,00 32,12 32:24
rilatS975810 tl-430 AcqtlO-SEP-1997 22,27,32 EH- Voltayu SIS 70S
479.7165 F,4 ExpiEPCUS
TRIANGLE LABS T*xt:O-M23-2 TLIt43057 XK7. TIME - 22,30
32:36
32:48
80:
50:
40:
20:
o:
31,58
3112
311 09
^9.7X5
.7.8X5
.5.8X5
.3.9X5
.1.9X5
0.0X0
Tim,
-2.2E6
J..8X6
.1.3X6
.8.8X5
.4.4X5
0.0X0
^2.1X6
.1. 7X6
.1.2X6
.6.3X5
'•.4.1X5
0.0X0
3,50
-.6.8X3
.5.4X3
.4.1X3
.2.7X3
.1.4X3
31\12
31\24
3l',3s'
31148
32100
32112
32,24
32,36
32,48
0.0X0
Tim
153
-------
XleisS75H10 #1-130 AcqtJ.0-SEP-l.9y7 12127132 EH- Voltage SIM 70S NOif»,J71
433.7766 T,4 BSOB(356,30, -3.0) PKD(7,5,3,0.05\,1484.0,1.00\,T,T) ElpiEPCDS
TRIANGLE LABS Tmxt,0-M33-3 TLH43QS7 IXT. TIME • 23,30
100\ A4.93E4 A6.66X4
31iIS 3lt34 31i30 31,36 31,42 31,48 31,54 32,00 32,06 33,13 32,18 33,24 32,30
'llf,S975810 41-430 AcqilO-SSP-1997 22,27,32 CH- Voltag* SIS | 70S Noif»,385
435.7737 F>4 BSOB(356,30,-3.0) PKD(7,5,3,0.OS\,1140.0,1.00\,T,T) ExptEPCUS
TXIASGLS LABS T*xt,O-M33-3 TLH43057 JKT. TIMX - 23,30
10 04 A4.69E4 AH. 83X4
80.
so:
40.
30.
OJ
.33X3
A1.20X4
A1.21E4
'.0.0X0
Tlmi
-1.9X4
-1.5X4
.1.3X4
.7.7X3
'.3.8X3
.0.0X0
31,18 31,34 31,30 31,36 31,42 31,48 31,54 33,00 32,06 32,13 32,18
rlle,S975810 91-430 AcqslO-SXP-1997 22,27,33 SI+ Voltag* SIX 70S Hoim»,370
435.8169 T,4 gSUS(356,30,-3.0) fXD(7,5,3,0.05\, 1480.0,1.00*,>,T; ExptZPCUS
TRIANGLE LABS Ttat:O-M23-2 TLH43057 fXT. TIMX • 22,30
1004 A4.38E6
801
eo:
40.
30'.
32,34 33,30
31', IB 31,34 31,30 31,36 31,43 31,48 31,54 33,00 32,06 32,13 33,18
Tilm,S975810 H-430 Acq,10-SEP-1997 33,37,33 XII- Voltagr* SIS\70S Boia»,322
437.8140 f,4 BSV3(356,30,-3.0) PXD(7,5,3, 0.051,1388.0,1.00*,T,T) XXpiXPCtJS
TRIANGLE LABS T*xt,O-tO3-2 TLH43057 OKT. TIMX - 32,30
100\ A4.96X6
so:
601
40:
30.
.1.5X6
.1.3X6
19.0X5
.6.0X5
.3.0X5
0.0X0
33,24 32i30
3lil8 31,24 31,30 31,36 31,42 31,48 31,54 33,00 .
rll*iS975810 41-430 AcqtlO-SXP-1997 33,37,33 EH- Voltags SIS
430.9739 Tt4 ElptEPCVS
TRIANGLE LABS Tt*t,O-M33-3 TLH43057
1004 __ ._ ,,.3o 31/50
so:
60.
40.
20:
0.
31,29
31,18 31,34 31,30 31,36 31,42 31,48 31,54 32,00
2,06 33,13 33,18 33\34 ' '32,30
70S
.IV. TOO! - 33,30
32:13
-1.4X6
.1.1X6
.8.6X5
.5.7X5
'.3.9X5
0.0X0
-3.0X6
'-1.6X6
'.1.3X6
.7.9X5
.4.0X5
.0.0X0
V,06 33,12 33,18 32,34 32,30
134
-------
rile.-SS758.10 tl-430 AcqsJ.0-SEP-J.997 22>27i32 EJ-f Voltage SIM 70S KOif»>43
141.7428 Tt4 BSVB(256,30, -3.0) PKD(7,Sr3,0.05\,172.0r1.00\,T,T) XxptEPCOS
TSIASGLS LASS Text:O-M23-2 TLII43057 OKT. TIME - 22t30
1001
31:00 32:00 33:00 34:00
rile:SS75810 tl-430 AcqsJ.0-SEP-J.997 22t27:32 SH- Valtaff* SIS 70S Soimm»34
443.7399 r,4 BSUB(256,30,-3.0) PXD(7,5,3,0.05\,136.0,1.00\,r,T) XxptEPCOS
TRIANGLE LASS Tejct:O-H23-2 TLH43057 OKT. TIMS • 22i30
100\
35100
A1.17S4
A1.20S4 A7.61
4.87X3
31:00 32:00 33:00 34:00
Tile:S975B10 tl-430 Acq:10-SEP-1997 22:27:32 EI+ Valtay* SIM 70S
430.9729 f:4 Exp:EPCUS
TSIANGLE LABS T«xt:0-M23-2 TLH43057 HOT. TIMS - 22:30
1001
35s 00
31:00 32', 00 33:00 34:00
rile:S97SaiO tl-430 AcqilO-SEP-1997 22t27t32 ZI+ Voltage SIS 70S
513.6775 fs4 Exp:£PCOS
TSIAKSLZ LABS TextsO-H23-2 TLH43057 ISJ. TIHS -
ion
901
aoj
701
601
501
401
301
201
101
0.
35:00
22130
33:58
34:48
30:45
31 tOO
32:00
33:00
34:00
35:00
155
-------
Lmsay/3UJ.U n-uo AcqtJ.u-SEp-j.yy/ jjtj/»jj EH- voicay* SIM 70S
457.7377 r,4 BSUB(256,30,-3. 0) tO>(7,5,3,0.05\f132.0,1.00\,T,T) XfpiXPCOS
TRIANGLE LABS T*xtiO-M23-2 TLH43057 1X7. TIMS -
1001 AS. 09X4
34,24 34i30 34:36 34,42 34,48
r±l*,S975810 tl-430 AcqtlO-SXP-1997 22,27,32 XI+ Volttgm SIX 70S Koim»,28
459.7348 T:4 BSUB(256,30,-3.0) PXD(7,5,3,0.051,112.0,1.00\,F,T) XxftXPCOS
TRIANGLE LABS T»xtnO-M23-2 TLH43057 XK7. TOO! -
34,24 34,30 34,36 34,42 34,48 34,54
TileiSS75810 tl-430 AcqtlO-SEP-1997 22i27t32 EI+ Voltaga SIX 70S Noifm>20
469.7779 Ti4 BSDB(256,30,-3.0) PXD(7,5,3,0.051,80.0,1.00\,r,X) SxptSPCUS
T&IANGLE LABS T«xtiO-H23-2 TLH43057 OKT. ZZXK - 22,30
1001 A3.Q2X6
22i30
34,54
22,30
100S
80.
60.
40.
20.
A8.94E4
A4.31E3
A8.51X3
/\
.0.0X0
35 tOO H»«
.2.114
.1.7X4
.1.3X4
.8.4X3
.4.2X3
34:24 34', 30 34,36 34t42 34,48 34,54
Fila,3975810 tl-430 AcqslO-SEP-1997 22,27,32 EH- Voltag* SIX 70S Noifts29
471.7750 Fs4 BSUX(256,30,-3.0) PKD(7,5,3, 0. 05»,115.0,1.00\,r,T) ExpiEPCVS
TRIAKSUS LABS T«xtIO-M23-2 TLH43057 IKJ. TIME - 22,30
1003
80.
601
40.
20:
A3.49E6
34154
34', 24 34',30 . 34,36 34,42 34,48
rile,S97S810 tl-430 AcqtlO-SEP-1997 22,27,32 XX* Volt*g* SIX 70S
430.9729 T:4 XxpiXPCtJS
TRIANGLE LABS T*xt.,O-M23-2 TLIt43057 IKJ. TIME - 22,30
lOOi
80.
60.
40.
201
o:
34,24
34:33
.0.0X0
35100 T±m»
.6.6X5
.5.3X5
.4.0X5
J.7X5
.1.3X5
.0.0X0
35100 Time
-.7.9X5
.6.3X5
.4. 7X5
.3.2X5
Ll. 6X5
.0.0X0
35100 TiMm
34,58 -2.2X6
*^
'.1.7X6
.1.3X6
.8.7X5
.4.4X3
0.0X0
34,24
34130
34,36
34142
34148
34154
35 tOO
156
-------
fe?, MSS 282.385 Pe-k top
*ight i.14-wits Span 298 ppi
Oa fits nae
EPCUS2
A-S9US71
2
Icnizaticn Kxfe EI-
Swltchuig VOLTRGE
tef, lasses 292,9825, 416,9768
J 331
K 332
L 334
K 348
N 342
0 352
P 354
fl 356
R 358
293
3 384
C 386
0 316
E 318
f 328
G 322
H 328
3 368
T 378
II 376
V 418
I 331
Channel I 338.3792 Peak top
1,41 wolts Span 288 opt
157
-------
NJ *».
-------
en
ID
File:S975810 #1-405 Acq:"10-SEP-1997 22:27:32 EI+ Voltage SIR 70S
389.8156 F:3 Exp:EPCUS
Sample Text:O-M23-2 TLI#43057 INJ. TIME -
1004 . A3.55E4
80 j
60:
40J
20:
22:30 File Text:O-M23-2 TLI#4»
2.0E4
L1.6E4
L1.2E4
i.8. OE3
_4.0E3
28:48 28:54 29:00 29:06 29:12 29:18 29:24 29:30 29:36 29:42 29:48 29:54 30:00
O.OEO
Time
File:S975810 #1-405 Acq:10-SEP-1997 22:27:32 EI+ Voltage SIR 70S
391.8127 F:3 Exp:EPCUS
Sample Text:O-M23-2 TLI#43057 INJ. TIME -
1001 A3.72E4
80:
60 j
40:
20 j
22:30 File Text:O-M23-2 TLI#4»
1.8E4
L1.4E4
L1.1E4
_7.1E3
_3.5E3
28:48 28:54 29:00 29:06 29:12 29:18 29:24 29:30 29:36 29:42 29:48 29:54 30:00
O.OEO
Time
File:S975810 #1-405 Acq:10-SEP-1997 22:27:32 EI+ Voltage SIR 70S
401.8558 F:3 Exp:EPCUS
Sample Text:0-M23-2 TLI#43057 INJ. TIME =
100%, 29; 31
60:
40 j
20 j
Oj
29:09
29:14
22:30 File Text:O-M23-2 TLI#4>
5.0E6
L4.0E6
-3.0E6
.2.0E6
_9.9E5
llilllli|lllli|lliiifiirii|iiiiT[iiiii[iliri|iiii T"| i I I I I | I I i i i [ i i i i I | I i i i i i i i
28:48 28:54 29:00 29:06 29:12 29:18 29:24 29:30 29:36 29:42 29:48 29:54 30:00
O.OEO
Time
-------
File:S975810 #1-430 Acq:10-SEP-1997
407.7818 P:4 Exp:EPCUS
Sample Text:0-M23-2 TLI#43057
lOOJ. A1.Q5E5
80 j
22:27:32 EI+ Voltage SIR 70S
INJ. TIME = 22:30 File Text:O-M23-2 TLI#4»
_3.7E4
31:48 32:00 32:12 32:24 32:36 32:48 33:00
31:00 31:12 31:24 31:36
File:S975810 #1-430 Acq:10-SEP-1997
409.7789 F:4 Exp:EPCUS
Sample Text:0-M23-2 TLI#43057
lOOi A1.20E5
22:27:32 EI+ Voltage SIR 70S
INJ. TIME =
22:30 File Text:0-M23-2 TLI#4»
,.4. 1E4
-,
i i—i—i [' 1 i—i 1*1—|—i
31:48 32:00 32:12 32:24 32:36 32:48 33:00
31100 31:12
File:S975810 #1-430 Acq:10-SEP-1997
417.8253 F:4 Exp:EPCUS
Sample Text:O-M23-2 TLI#43057
lOOi 31;13
60 J
40J
20 j
OJ
T—I—I I I—I I I
31:00
22:27:32 EI+ Voltage SIR 70S
INJ. TIME =
32:25
31:12
i r i i -i i i i i i—r
31:24 31:36
22:30 File Text:O-M23-2 TLI#4>
9.7E5
L7.8E5
L5.8E5
_3.9E5
.1.9E5
O.OEO
iiiiiiiiiirTiiiiiiifii P'I i i -i i i i i i i i • i i i—i i i i i
31:48 32:00 32:12 32:24 32:36 32:48 33:00 Time
O
CD
-------
191
ro «n o -H
a a w w w
H VO O
-------
TLI Project:
Client Sample:
43057
O-M23-2
Method 23 TCDD/TCDF Analysis (DB-225)
Analysis File: P973845
Client Project:
Sample Matrix:
TLI ID:
Sample Size:
Dry Weight
GC Column:
ASPHALT •PLANT" ft"
M23TRAIN
181-27-3A-C
1.000
n/a
DB-225
Date Received:
Date Extracted:
Date Analyzed:
Dilution Factor
Blank File:
Analyst
08/29/97
09/06/97
09/12/97
n/a
S975807
WK
Spike File:
ICal:
ConCal:
% Moisture:
%Lipid:
% Solids:
SPC2NFD4
PF22206
P973843
n/a
n/a
n/a
2^,7,8-TCDF
•X:,r2,3,7,8-TCDF
ND
0.02
2.1
52,4
409b-130%
0.76 20:42
0.79 19:44
Data Reviewer.
Page I of 1
09/12/97
C2NF_pa «2JDO. LAIS & HUM
Triangle Laboratories, Inc.*
801 Capitola Drive • Durham, North Carolina 27713
Phone: (919) 544-5729 • Fax: (919) 544-5491
Printed: 1457 09/12/97
-------
Initial
Data Review By:
Date...
^ I- T ^
•* j i ^ '
Calculated Noiae Area:
2.11
The Total Area for each peak with an ion abundance ratio outside
ratio limits has been recalculated according to method requirements.
Page No.
09/12/97
Listing of P973845B.dbf
Matched GC Peaks / Ratio / Ret. Time
Compound/
M_Z.... QC.Log Omit Why ..RT. OK Ratio Total.Area... Area.Peak.1.. Area.Peak.2.. Rel.RT Conpound.Na»e.. ID.. Flags.
TCDF
304-306
304-306
13C12-TCDF
316-318
316-318
13C12-TCDD
332-334
0.65-0.89
DC NL 0:00 0.85
DC SN 19:03 RO 1.22
DC
DC
DC
DC
DC
DC
DC
DC
DC
DC
DC
SN
SN
0
NL
WL
SN
WH
1
NL
SN
SN
SN
WH
19
20
:26
:42
RO
RO
1.
1.
16
09
Peaks
0
19
20
21
22
:00
:27
:42
:38
-.34
0
RO
RO
RO
.65-0.89
1.
1.
0.
0.
0.
11
01
76
78
29
Peak
0
19
19
19
20
20
20
21
:00
:01
:31
:44
:24
:29
:58
:45
0
RO
RO
RO
RO
RO
.65-0.89
1.
1.
0.
0.
0.
2.
0.
2.
38
48
79
79
82
62
22
27
3.17
3.26
2.28
3.08
0.00
2.51
4.18
1,088.09 469.12
1.98
3.79
1,088.09
Above: TCDF / TCDD Follows -
0.786-1.096
0.000
0.920
0.939
1.000 2378-TCDF
AM
0.952-1.048
0.000
0.940
618.97 1.000 13C12-2378-TCDF ISO
1.04S
1.090
332-334
3 Peaks
2.58
1.95
832.51 367.79
1,495.20 661.22
11.35 5.10
0.65
0.71
1.91
2,339.06
0.897-1.103
0.000
0.974
464.72 1.000 13C12-2378-TCDD IS1
833.98 1.011 13C12-1234-TCDD RSI
6.25 1.045
1.050
1.074
1.114
Column Description -Why* Code Description QC Log Des =.
M_Z -Nominal Ion Mass(es) WL-Below Retention Time Window A-Peak Added
..RT. -Retention Tine (mo:sa) WH-Above Retention Tine Window K-PeaJe Kept
Rat.l -Ratio of M/M+2 Ions SN-Below Signal to Noise Level D-Peak Deleted
OK -RO-Ratio Outside Limits
-------
303.9016 BSUB(256,30,-3.0) PKD(5,3,1,0.10\,
XBIMKLZ LASS TaxtiO-H23-2 TLH43057
1001
17iOO 18tOO 19i00 20i00 21iOO
Til»iP973845 fl-755 Acqil2-SSP-1997 12t43i29 XI* Volt*?* SIS 7OP Koim»,856
305.8987 BSUB(256,30,-3.0) PXD(5,3,1,0.10\,3424.0,0.00\,r,f) Xxp,DB225
TXIANGLZ LAIS TextiO-M23-2 XLIt43057
1001
22iOO
17,00 18,00 19,00 20,00 21iOO
rll9,P973845 #1-755 Acq,12-SfP-1997 12>45t29 XI+ Volttgm SIX 7OP Bo±emi788
315.9419 BSUB(256,30,-3.0) PKD(S,3,1,0.101,3152.0,0.00\,r,T) BcptDB225
TRIANGLE LABS T*XttO-M23-2 TLX+43057
1001 A«.<
80.
60.
40.
20.
22,00
17,00 10>00 19(00
FileiP973845 41-755 Acqtl2-SEP-1997 12,45,29 EI+ Voltag* SIX 70P Wbi**t712
317.9389 BSUB(2S6,30,-3.0) PXO(5,3,1, 0.10\,2848. 0,0.00\,T,T) Exp,DB225
TRIANGLE LABS T*xt.:0-K23-2 TLH43057
1001 A6.J.9S6
80.
60.
40.
20.
22100
17,00 18,00 19(00
rll»,P97384S H-755 Acq,12-BKP-1997 12145139 JX+
375.8364 Exp,DB22S
TRIAJKLX LASS T*xtiO-M23-2 TLHM3037
100*16,27
80.
60.
40.
20.
0.
30.00 21,00
ga TOP
22,00
adit 20i50
0.0X0
'.0.0X0
Timm
.1.316
'.1.0X6
-7.7X5
15.1X5
Lfl.OEO
.1.3X6
.9.6X5
.6.4X5
.3.2X5
0.0X0
T±mm
22(00 22(40
^5.1X4
.4.1X4
.3.0X4
.2.0X4
.1.0X4
'.0.0X0
17,00
10(00
19100
20100
31100
22 tOO
164
-------
tl-755 Acq,13-SEP-l997 12,45,39 E14- Voltage SIS 70P Voi**tt>70
319.8965 BSOB(256,30,-3.0) PKD(5 , 3,1,0.10\,26BO .0,0.00\,F,r) XxpiDB225
TRIANGLE LABS TfJttlO-M23-2 TLH430S7
100\A1.93E4
80.
60.
40.
'ISiOO19iOO 20i00 21iOO
T±letP973845 tl-755 Acqil2-SEP-1997 12t45i29 EH- Voltagm SIS 70P Koim»t74f
321.8936 BSOB(256,30,-3.0) PXD(5, 3,1, 0.10\, 2984.0, 0.00\,r,f) ElptDB225
TXIAHSLX LABS XexttO-M23-2 TLH430S7
100\A2.66X4
22tOO
801
60.
40.
20:
01
A3.07X3
A4.45X3
19 \ 00 20100 21100
rilotP973845 tl-755 Acqil3-SXP-1997 12t45t29 EI+ Volt*9» SIX 70P Solm»i854
327.8847 BSOB(256,30,-3.0) PKD(5,3,1, 0.10\,3416.0,0.00\,t,t) ErpiDB225
TXIAOGLX LABS T*xt>0-H23-2 TLH430S7
1001 A6.97X6
801
60.
401
20.
22100
OJ
IStOO 19tOO 20i00
r±letP973845 tl-755 Acqtl2-SEP-1997 12145129 EH- Voltmgm SIX 70P BOi»»tl009
331.9368 BSUB(256,30,-3.0) PXD(5,3,1, 0.10\,4036.0, 0.00\,I,T) ExptDB225
TRIANGLE LABS Taxt:0-M23-2 TLH43057
1001 A6.61X6
22>»0
801
601
401
201
A3.68X1
18,00 19i00 20i00
rile,P973845 tl-755 Aoqtl2-SXP-1997 12i45i29 EI+ Voltmg* SIX 70P Hol*m:729
333.9338 BSUB(256r30,-3.0) PKD(5,3,1, 0.10\,2916.0, 0.00\,T,T} XxptDB225
TXIASGLX LABS T*xttO-H23-2 XLIt43057
1001 AS. 34X6
801
601
401
22100
201
01
A4.65Xi
10100
15100
20100
Jit 00
f1.0X4
'.8.0E3
.6.0X3
.4.0X3
.2.0X3
0.0X0
ZiMJ
.8.9X3
.6.7X3
.4.4X3
.2.2X3
0.0X0
.1.4X5
.1.1X6
.7.2X5
.3.6X3
0.0X0
Urn*
. 4X6
.1.1X6
.7.1X5
.3.5X5
0.0X0
Urn,
-3.3X6
JL.8X6
.4X6
.4.6X5
o.oxo
22100
165
-------
•iletP973845 tl-755 Acqtl2-SEP-1997 12:45:29 EI+ Voltage SIX 70P
303.9016 Xxp:DB225
TRIANGLE LABS T*JCt: 0-M23-2 TLH43057
17t00 18:00 19iOO 20:00 21:00
r±leiP973845 tl-755 Aoqil2-SXP-1997 12:45:29 11+ Voltage SIX 701
315.9419 Exp:DB225
TXIAKGLX LABS Textl 0-M23-2 TLIf43057
1001 20142
80:
60:
40:
20:
17:00 18:00 19:00 20:00 21:00
r±lfiP973845 tl-755 Acqtl2-SXP-1997 12:45:39 11+ Voltage SIX 70P
319.8965 Eip:DB225
TRIANGLE LABS TexttO-M23-2 TLIt43057
22 tOO
22100
17:00 18:00 19:00
r±lmtP973S45 tl-755 Aoq:12-SXP-1997 12:45:29
331.9368 KzpiDB225
TSIAHGLX LASS TexttO-M23-2 STMJ057
1001
flOj
50J
401
20J.
ol
20:00 21100
voltage SIX 7«P
If
191
17:00 18:00
ril»>P973845 tl-755
292.9825 Xxp>DB225
TSIASSLX LASS TmxttO-H23-2
17117 17,42
60.
40:
20.
o:
19tOO 20100
12:45i29 ZT+ Voltfym MTX 70P
21:00
TLH43057
18:3719:01
20101
21*57
17:00 18:00 19:00 20:00 21:00
ril»:P973845 tl-755 Acgtl2-SXP-1997 13:45:29 EH- Voltage SIX 70P
330.9792 EipiDB225
TXIA1KLX LASS T*zt:0-M23-2 TLIt43057
100^.- 16:44 17il7 17,48 la.11 18t4» 19t53
, •** - /v»vu*v -
80:
60:
40:
20:
o:
22:00
21153
.1.3 ft
.1. 0X6
.7.7X5
.5.2X5
.2.6X5
,0.0X0
Tin.
.7.1X5
'•.3.6X5
0.0X0
Tim,
.8.axe
'-.7.1X6
.5.3X6
.3.5X6
.1.8X6
.0.0X0
.9.7X6
.7.8X6
.5.8X6
.3.9X6
'•.1.9X6
17100
18:00
19:00
20:00
21100
LO.OXO
timm
166
-------
Ref, lass 292,3825 Peak top
Height 1.33 volts Span 286 ppi
System file naie
Data file naie
Resolution
Group nuaber
lonlzatlon iode
Sultching
Ref, lasses 292.9825,
292.9825
383,9616
315.9419
317.9389
319.8965
321.8936
327.8847
336.9792
J
K
L
I
fl'P973845
18688
1
El*
VQLTRGE
388.9761
338.9792
331.9368
333.9338
375.8364
Channel I 338.9792 Peak top
Height 1.41 volts Span 286 ppi
167
-------
TLI Project: 43057
Client Sample: O-M23-3
Method 23 PCDD/PCDF Analysis (a)
Analysis File: S975811
Client Project:
Sample Matrix:
TLI ID:
Sample Size:
Dry Weight
GC Column:
/toWcr -**** "A"
M23TRAIN
181-27-4A-C
1.000
n/a
DB-5
Date Received:
Date Extracted:
Date Analyzed:
Dilution Factor
Blank File:
Analyst
08/29/97
09/06/97
09/10/97
n/a
S975807
ML
Spike File:
ICal:
ConCal:
% Moisture:
%Lipi±
% Solids:
SPX23704
SF56117
S975797
n/a
n/a
n/a
Analyses ; -' » f?'.
2,3,7,8-TCDD
1,2,3,7,8-PeCDD
1,23,4,7,8-HxCDD
1,2,3,6,7,8-HxCDD
1,2,3,7,8,9-HxCDD
1,2^,4,6,7,8-HpCDD
1,2^,4,6,7,8,9-OCDD
2,3,7,8-TCDF
1,23,7,8-PeCDF
2^.4,7,8-PeCDF
1,2^,4,7,8-HxCDF
1,2,3,6,7,8-HxCDF
2,3,4,6,7,8-HxCDF
1,2,3,7,8,9-HxCDF
1,2^,4,6,7,8-HpCDF
1,2,3,4,7,8,9-HpCDF
1,2,3,4,6,7,8,9-OCDF
vTA*4il4» > - -^ C % ^ ',•,*
lotats ^ *^\\ s'-s/vc
Total TCDD
Total PeCDD
Total HxCDD
Total HpCDD
Total TCDF
Total PeCDF
Total HxCDF
Total HpCDF
-- -' '*-, :\Asmt fa$ "}
FJ^lPC
0.005
0.008
0.02
EMPC
0.06
0.13
0.02
0.007
0.01
0.06
OD2
0.02
ND
OJ09
EMPC
0.06
*/s\v ',- "-.*- ABJ^^g^
0.01
0.03
0.15
0.06
0.03
0.06
0.17
0.09
? *
0.003
0.01
0003
0.03
"V^^ "V^^1** %S»L^;™ "."^'"/wSsps^
2 0.02
3 0.05
5 ai6
1 0.11
3 0.04
6 0.07
7
1 0.17
*{ ^'fte&^ll
1.49
1.10
1.41
0.80
0.73
1.61
L32
1.20
104
1JQ9
1JDO
0.82
^S^&A^-te.vW:ffl;^
^^ ^»^^^S^^^&^^
^^?]^^^
25:55
29:11
29:16
32:07
34:36
20:28
24:45
25:31
28:25
28^32
29:02
31:16
34:42
fig$g@gsjji&fi£S«9$SggK™^
9^^fS^^x
-------
Project:
:iient Sample:
43057
O-M23-3
Method 23 PCDD/PCDF Analysis (a)
Analysis File: S975811
Internal Standards Sft* •',
Ci2-2,3,7,8-TCDF
Ci2-2,3,7,8-TCDD
d2-lA3,7,8-PeCDF
d2-U,3,7,8-PeCDD
Ci2-lA3,6,7,8-HxCDF
C,2-1^3,6,7,8-HxCDD
C,2-lA3,4,6.7,8-HpCDF
C,2-lA3,4,6,7,8-HpCDD
Ci2-l,2,3,4,6,7,8,9-OCDD
% \ s Ami; {ngj;x ^ s
7.4
6.5
6.4
6.8
7^
6.9
4.2
4.4
5.2
#:, »ARecovei
184
163
161
170
187
173
105
109
65.1
40%-130%
40%-130%
409fc-130%
40%-130%
409b-130%
409b-130%
25%-130%
259b-130%
25%-130%
0.76
0.80
1.45
1.50
0^0
1-22
0.43
1.08
0.88
20:25
21:15
24:45
25:53
28:31
29:14
31:15
32:07
34:35
CU-2^,7,8-TCDD
Ci2-2,3,4,7,8-PeCDF
C.2-lA3,4,7,8-HxCDF
Ci2-lA3,4,7,8-HxCDD
C,rU,3,4,7,8,9-HpCDF
3.9
3.9
3.5
3.7
98.4
88.6
98.2
87.9
91.3
70%-140%
70%-140%
70%-140%
709fe-140%
70%-140%
1.45
0.50
0.40
21:16
25:31
28:24
29:10
32:27
Ci2-lA3,7,8,9-HxCDF
C,r2,3,4,6,7,8-HxCDF
409b-130%
40%-130%
OJO
OJO
29:44
29:02
Recovery Standards;
CirU,3,4-TCDD
Ci2-l,2,3,7,8,9-HxCDD
0.80
1.21
21:02
29:32
Data Reviewer.
Page 2 of 2
09/12/97
'dangle Laboratories, Inc.*
01 Capitola Drive • Durham, North Carolina 27713
•hone: (919) 544-5729 • Fax: (919) 544-5491
Printed: 08:18 09/12/97
169
-------
Data Review By:
Date...
'__!_ (calculated Noise Area: 1.55
The Total Area for each peak with an ion abundance ratio outside
ratio limits has been recalculated according to method requirements.
Page No.
09/12/97
.Listing of S975811B.dbf
Hatched GC Peaks / Ratio / Ret. Time
Compound/
M_2.... QC.Log Omit Why ..RT. OK Ratio Total. Area. .. Area. Peak. 1.. Area.Peak.2.. Rel.RT Compound. Name.. ID.. Hags.
TCDF
304-306
D
D
D
A
M
D
304-306
13C12-TCDP
316-318
316-318
TCDD
320-322
D
MX
DC
DC
DC
DC
D
D
D
DC
D
DC
DC
DC
DC
DC
DC
D
DC
DC
DC
DC
DC
DC
NL
SN
SN
SN
SN
SN
SN
SN
SN
WH
5
NL
WL
3
NL
WL
SN
SN
SN
SN
SN
SN
SN
SN
0
17
17
17
18
:00
:24
:26
:43
:07
18:27
19
19
19
19
20
20
20
22
22
:17
:34
:44
:58
:15
:28
:56
:21
:38
0.
RO
RO
RO
RO
RO
RO
RO
RO
65-0.89
1
1
2
0
0
1
0
0
0
0
0
0
1
0
0
.14
.84
.19
.48
.89
.01
.68
.81
.72
.95
.77
.73
.00
.90
.88
Peaks
0
19
19
20
20
:00
:15
:57
:25
:55
0.
RO
RO
0.
0.
2.
4.
7.
12.
14.
17.
10.
35.
6.
65.
9.
17.
2.
147.
12
80
00
71
30
55
25
93 8.01
72 4.47
86 19.29
36
40 27.55
77
13 8.67
76
04
65-0.89
5
0
0
0
1
Peaks
0
18
18
18
18
19
20
20
20
20
21
21
:00
:08
:22
:40
:51
:55
:14
:26
-.40
:47
:00
:08
21:17
DC
DC
SN
SN
21
22
:36
:24
0.
RO
RO
RO
RO
RO
RO
RO
RO
RO
RO
.88
.84
.89
.7* H,
.11
11,
0.
17.
48.
230.
35.
314.
mtf*rvm
14
19
30 22.68
27 4.K33.7*
82 22.4C
39
65-0.89
1
1
0
1
0
0
1
2
0
0
0
2
0
0
0
.17
.00
.84
.17
.68
.84
.01
.69
.63
.67
.74
.10
.38
.49
.98
0.
0.
20.
0.
9.
7.
1.
3.
2.
1.
2.
2.
5.
1.
1.
11
37
83 9.48
94
52 3.85
63
79
40
46
10
56
53
98 2.80
06
03
0.823-1.104
9.92
6.25
20.26
37.85
9.68
0.000
0.852
0.854
0.868
0.887
0.904
0.944
0.958
0.967
0.978
0.992
1.002 2378-TCDF AN
1.025
1.095
1.109
0.951-1.049
25.62
C,3M.48
20.24
0.000
0.943
0.977
l.OOO 13C12-337B-5CDF ISO
1.024
0.857-1.061
11.35
5.67
6.81
0.000
0.853
0.8*4
0.878
0.887
0.937
0.952
0.962
0.973
0.978
0.988
0.995
1.002 2378 -TCDD AN
1.016
1.054
Triangle Laboratories, Inc.® Analytical Services Division
801 Capitola Drive • Durham, North Carolina 27713
Phone: (919) 544-5729 • Fax: (919) 544-5491
Printed: 08:18 09/12/97
170
-------
Page No.
09/12/97
Listing of S975811B.dbf
Matched GC Peaks / Ratio / Ret. Tine
Compound/
M_Z.... QC.Log Omit Why ..RT. OK Ratio Total.Area... Area.Peak.1.. Area.Peak.2. . Rel.RT Compound.Hue.. ID.. Flag*.
320-322
3 Peaks
36.33
37C1-TCDD
328
328
13C12-TCDD
332-334
332-334
PeCDF
340-342
D
D
D
A
A
AN
D
D
340-342
13C13- PeCDF
352-354
352-354
DC NL 0:00
19:42
21:16
2 Peaks
DC NL 0:00
19:55
21:02
21:15
21:38
4 Peaks
DC NL 0:00
DC SN 22:30
22:39
DC SN 22:53
DC SN 23 : 18
D SN 23:43
23:51
D SN 24:02
D SN 24 : 12
24:25
24:40
24:45
DC SN 24 : 57
25:04
25:31
D SN 25:41
DC SN 25 : 59
D SN 26:31
DC SN 26 : 38
7 Peaks
DC NL 0:00
23:51
24:23
24:45
24:56
25:04
25:31
26:30
7 Peaks
0.
RO
RO
RO
65-0.89
11.11
0.90
0.80
0.80
0.93
0.
12.
6,682.
6,694.
0.
38.
4,631.
8,057.
115.
06
62
06
68
16
25
87
34
35
12,842.81
1.
RO
RO
RO
RO
RO
RO
RO
RO
RO
RO
1.
RO
RO
32-1.78
0.89
0.68
1.64
0.30
0.61
1.25
1.34
1.40
1.36
1.39
1.92
1.61
1.18
1.36
1.32
1.51
0.67
2.18
1.04
32-1.78
1.00
1.61
1.33
1.45
0.93
1.36
1.45
1.49
0.
1.
15.
0.
0.
8.
41.
8.
7.
36.
13.
16.
5.
14.
28.
15.
3.
8.
1.
166.
0.
36.
42.
8,446.
27.
55.
7,255.
15.
15,880.
13
84
92
41
73
67
00
29
91
10
92
68
00
32
52
93
69
13
25
46
12
62
06
74
98
81
87
15
23
12.62
6,682.06
19
2,054
3,572
60
.55
.00
.72
.39
21.
2,577.
4,484.
65.
0.906-1.094
0.000
0.927
1.001 37C1-TCDD
0.906-1.094
61
87
62
17
0.000
0.937
0.990 13C12-1234-TCDD
1.000 13C12-2378-TCDD
1.018
SOR1
RSI
IS1
CDF Follows
9
23
21
10
10
8
16
22
23
5,005
17
32
4,294
9
.89
.45
.00
.50
.30
.25
.23
.57
.97
.88
.01
.18
.07
.06
6.
17.
15.
5.
6.
6.
12.
14.
18.
3,440.
18.
23.
2,961.
6.
0.909-1.079
03
55
10
46
38
07
29
0.
05
09
86
20
63
80
09
0.000
0.909
0.915
0.925
0.941
0.958
0.964
0.971
0.978
0.987
0.997
1.000 12378-PeCDF
1.008
1.013
1.031 23478-PeCDF
1.038
1.050
1.071
1.076
838-1.162
0.000
0.964
0.985
1.000 13C12- PeCDF 123
1.007
1.013
1.031 13C12- PeCDF 234
1.071
AN
AN
IS2
SOR2
Triangle Laboratories, Inc.® Analytical Services Division
801 Capitola Drive • Durham, North Carolina 27713
Phone: (919) 544-5729 • Fax: (919) 544-5491
Printed: 08:18 09/12/97
171
-------
Page No.
09/12/97
Listing of S975811B.dbf
Matched GC Peaks / Ratio / Ret. Tlae
Compound/
M_Z QC.Log Omit Why ..RT. OK Ratio Total.Area... Area.Peak.1.. Area.Peak.2.. Rel.RT Compound.Name.. ID.. Flags.
PeCDD
356-358
K
356-358
13C12- PeCDD
368-370
368-370
HxCDF
374-376
D
D
D
374-376
13C12-HXCDF
384-386
384-386
DC NL 0
24
DC SN 24
DC SN 24
24
DC SN 24
25
25
DC SN 26
DC SN 26
:00
:00
:12
:31
:47
:54
:06
:55
:03
:22
1.
RO
RO
RO
RO
RO
32
1
0
1
2
1
1
1
1
0
0
-- Above
-1.78
.33
.75
.41
.13
.51
.04
.59
.49
.90
.96
4 Peaks
DC NL 0
DC SN 24
25
26
:00
:48
:53
:02
1.
RO
: PeCDF /
0.14
18.34
1.66
1.58
26.98
2.47
19.78
7.06
2.29
3.24
72.16
PeCDD Follows
11
16
12
4
.15
.21
.15
.22
14.
10.
7.
2.
32-1.78
1
1
1
1
2 Peaks
DC NL 0
27
27
27
28
28
28
D SN 28
D SN 28
29
DC SN 29
D SN 29
DC WH 30
DC WH 30
DC WH 30
:00
:25
:34
:53
-.03
:25
:32
:38
:51
:02
:10
:51
:10
:12
:17
1.
RO
RO
RO
RO
RO
RO
.17
.38
.50
.52
0.12
5.26
4,994.81
457.99
5,452.80
**_***^n t
05-1.43
1
1
1
1
1
1
1
1
1
1
0
0
1
0
1
.87
.18
.15
.31
.31
.20
.14
.42
.19
.09
.39
.97
.54
.55
.44
7 Peaks
DC NL 0
27
28
28
29
29
:00
:35
:24
:31
:02
-.44
0.
RO
43
0
0
0
0
0
0
-0.59
.29
.47
.50
.50
.50
.50
5 Peaks
2.60
29.45
60.86
12.18
9.11
87.48
37.44
9.37
11.62
38.17
1.07
14.22
0.87
0.74
2.67
274 . 69
1.66
11.85
4,748.79
5,041.60
4,322.80
2,605.10
1C, 730. 14
2,999
276
.63
.47
1,995.
181.
0.921-1.026
0.000
78 0.927
0.935
0.947
77 0.958
0.962
63 0.970
84 1.001 12378-PeCDD
1.006
1.019
0.845-1.155
0.000
0.958
18 1.000 13C12- PeCDD 123
52 1.006
AM
IS3
IS
.93
32.57
6
5
47
19
19
1
1,587
1,680
1,442
863
.91
.17
.75
.94
.94
.79
.75
.96
.18
.60
13.
28.
5.
3.
39.
17.
18.
8.
3,161.
3,360.
2,880.
1,741.
0.957-1.053
0.000
52 0.961
29 0.967
27 0.978
94 0.984
73 0.996 12347B-*zCDF
50 1.001 12367B-JUCQF
1.004
1.012
23 1.018 234678-HxCDT
1.023
1.047
1.058
1.059
1.062
0.859-1.141
0.000
06 0.967
04 0.996 13C12-HXCDF 478
64 1.000 13C12-HxCCF 678
62 1.018 13C12-HXCDF 234
50 1.043 13C12-HXCDF 789
AH
AH
AN
SDR3
IS4
ALT2
ALT1
Triangle Laboratories, Inc.® Analytical Services Division
801 Capitola Drive • Durham, North Carolina 27713
Phone: (919) 544-5729 • Fax: (919) 544-5491
Printed: 08:18 09/12/97
172
-------
Page No.
09/12/97
Listing of S97S811B.dbf
Matched GC Peaks / Ratio / Ret. Tiae
Compound/
M_Z QC.Log Omit Why ..RT. OK Ratio Total.Area... Area.Peak.1.. Area.Peak.2. . Rel.RT Compound.Name.. ID.. Flags.
HxCDD
390-392
M
390-392
13C12-HXCDD
402-404
402-404
DC NL 0
DC SN 27
27
DC SM 28
DC SN 28
28
28
29
29
29
DC WH 29
DC WH 29
:00
:49
:S7
:05
:14
:25
:39
:11
:16
:32
:S1
:S6
1.05
RO 1
RO 1
1
RO 0
RO 1
1
1
1
1
RO 0
1
RO 2
-- Abov
-1.43
.69
.92
.12
.80
.02
.34
.06
.10
.41
.93
.06
.27
6 Peaks
e: HXCDF / HXCDD FOJ.J.OWA --
1.68
1.12
11.13 5.87
1.08
1.07
81.45 46.69
34
7
18
15
0
0
167
.17 17.63
.34 3.85
.22 10.65
.50 8.58
.74
.83
.81
1.05-1.43
DC NL 0
28
29
29
29
DC SN 29
DC SN 29
:00
:38
:10
:14
:32
:4S
:45
RO 0
1
1
1
1
RO 0
1
.76
.32
.25
.22
.21
.21
.07
4 Peaks
1
15
3,306
3,863
2,240
0
3
9,425
.55
.50 8.83
.01 1,838.10
.39 2,122.72
.36 1,225.15
.83
.39
.26
n / Un/Ttf BV»1 1 nw« . -
0.951-1.015
0.000
0.952
5.26 0.956
0.961
0.966
34.76 0.972
16.55
3.49
7.57
9.20
0.
6.67
1,467.91
1,740.67
1,015.21
0.
0.
1.
1.
1.
1.
980
998
001
010
021
024
1234 78 -HxCDD
123678-HxCDD
123789 -HxCDD
AN
AN
AN
966-1.034
0.
0.
0.
1.
1.
1.
1.
000
979
998
000
010
018
018
13C12- HxCDD 478
13C12-HXCDD 678
13C12-HXCDD 789
SDR4
135
RS2
PR
HpCDF
408-410
M
M
408-410
13C12-HpCDF
418-420
418-420
HpCDD
424-426
DC NL 0:
31:
31:
31:
DC SN 31 :
32:
00
16
29
37
53
29
0.
RO
RO
RO
RO
RO
88-1.20
1
1
1
1
1
1
.94
.00
.30
.21
.22
.37
4 Peaks
DC NL 0:
31:
DC SN 31:
32:
00
15
34
27
0.
RO
RO
1
70
14
22
1
15
124
.67
.60 35.30
.99 9.52
.73 13.53
.29
.81 10.60
.13
37-0.51
1
0
0
0
2 Peaks
DC NL 0:
DC WL 31:
DC SN 31:
31:
00
15
23
31
0,
RO
RO
.88
1
2
1
0
.14
.43
.94
.40
-1.20
.00
.83
.00
.78
1
2,076
1
1,462
.31
.79 620.98
.89
.44 417.67
0.
35.30
7.35
11.14
7.75
0.
1,455.81
1,044.77
995-1.045
0
1
1
1
1
1
.000
.001 1234678-HpCDF
.007
.012
.020
.039 1234789-HpCDF
AN
AN
936-1.128
0
1
1
1
.000
.000 13C12-HpCDF 678
.010
.038 13C12-HDCDF 789
IS6
SOBS
3,539.23
0
3
1
24
.12
.28
.52
.26 12.37
0.
977-1.006
0
0
0
15.89 0
.000
.973
.977
.981
FB
Triangle Laboratories, Inc.® Analytical Services Division
801 Capitola Drive • Durham, North Carolina 27713
Phone: (919) 544-5729 • Fax: (919) 544-5491
Printed: 08:18 09/12/97
173
-------
Page No. 5 Listing of S975811B.dbf
09/12/97 Matched GC Peaks / Ratio / Ret. Tine
Compound/
M_Z.... QC.Log Omit Why ..RT. OK Ratio Total.Area. . . Area.Peak.1.. Area.Peak.2. . Rel.RT Compound. Huge.. ID..
0.991
17.20 16.40 1.000 1234678-HpCDD AH
1.010
0.969-1.031
0.000
0.981
1,032.68 960.55 1.000 13C12-HpCDD 678 IS7
1.006
M
424-426
13C12-HpCDD
436-438
436-438
OCDF
442-444
442-444
OCDD
458-460
458-460
13C12-OCDD
470-472
DC
SN
31
:49
32:07
DC
DC
DC
DC
DC
DC
DC
DC
DC
DC
DC
DC
DC
DC
DC
DC
DC
DC
DC
DC
DC
DC
DC
DC
DC
DC
WH
2
NL
SN
SN
1
NL
SN
SN
SN
SN
SN
SN
SN
SN
SN
SN
SN
SN
SN
SN
SN
SN
1
NL
SN
SN
1
NL
WH
32:27
RO
0.
1.
2.
89
05
44
Peaks
0
31
32
32
:00
:31
:07
:19
0.
RO
RO
88-
1.
1.
1.
0.
Peak
0
30
31
31
31
31
32
32
32
33
33
33
34
34
34
34
35
35
:00
:45
:01
:16
:40
:49
:00
:16
:44
:01
:17
:59
:24
:29
:42
:56
:20
:35
0.
RO
RO
RO
RO
RO
RO
RO
RO
RO
RO
RO
RO
RO
1.20
33
11
08
79
1.
33.
3.
57.
2.
4.
1,993.
3.
1,993.
t*.>s*v\m
76-1.02
0.
3.
1.
1.
0.
0.
0.
0.
10.
1.
1.
0.
0.
1.
25
21
25
78
93
14
15
32
86
81
39
74
55
76
0.82
RO
RO
RO
1.20
0.46
0.33
Peak
0
34
34
34
:00
:24
:36
:54
0.
RO
RO
RO
0.
0.
0.
0.
2.
0.
0.
0.
0.
0.
1.
0.
0.
0.
IB.
1.
1.
0.
IB.
08
60
12
86
18
93
23
02
23
15
45
68
87
26
21
30
47
13
59
34
49
59
85
35
34
13
81
as
76-1.02
1.17
1.34
0.
2.
80
.15
Peak
0:00
34
34
:35
:55
0.
RO
RO
0.11
1.06
2C.24
0.25
26.24
76-1.02
1.33
0,
.88
0.51
0.11
1,514.
.41
1.44
Follows
0.884-1.116
0.000
0.889
0.897
0.904
0.916
0.920
0.925
0.933
0.947
0.955
0.962
0.983
0.995
0.997
8.27 10.08 1.003 OCOF Ml
1.010
1.022
1.029
0.884-1.116
0.000
0.995
11.70 14.54 1.000 OCDD AN
1.009
0.996-1.005
0.000
7D«.B» 605.52 1.4)00 13C12-OCDD. IS8
1.010
470-472 1 Peak 1,514.41
Triangle Laboratories, Inc.® Analytical Services Division
801 Capitola Drive • Durham, North Carolina 27713 Printed: 08:18 09/12/97
Phone: (919) 544-5729 • Fax: (919) 544-5491 174,
-------
'age No.
19/12/97
Listing of S975811B.dbf
Matched OC Peak* / Ratio / Ret. Tine
Compound/
1_Z.... QC.Log Omit why ..RT. OK Ratio Total.Area... Area.Peak.1.. Area.Peak. 2.. Rel.RT Compound.Name.. ID.. Flags.
Zolumn Description "Why* Code Description QC Log Desc.
H_Z -Nominal loo Mass(es)
..RT. -Retention Time (mm:SB)
Rat.l -Ratio of M/m-2 Ions
OK -RO-Ratio Outside Linits
Rel.RT-Relative Retention Time
••* End of Report •••
WL-Below Retention Tine window
WH-Above Retention Time Window
SN-Below signal to Noise Level
-------
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r±l»:S975811 #1-848 Aoq:10-SEP-1997 23:06:56 EH- Voltagu SIS 70S No±ae:32
321.8936 Tt2 BSU3(256,30,-3.0) PKD(7,5,3,0.05\,128.0,1.00\,r,T) ElptEPCUS
TSIANSLE LABS TfxtsO-M23-3 TLH43057 IJKT. TIME - 23:09
1001
20iOO
Til»>S975811 #1-848 Aoq:10-SEP-1997 23:06:56 EI+ Voltayf SIS 70S HoimutSOO
331.9368 T:2 BSVB(256,30,-3.0) PKD(7,5,3,0.05\,2000.0,1.00\,T,T) ExptEPCOS
TRIANGLE LABS Tezt:O-M23-3 TLI#43057 HKT. TIME " 23:09
1001 A3
80:
60: A2.05X7
40:
20:
o:
19:00 20:00 21:00
TiletS975811 #1-848 AcqilO-srP-1997 23:06:56 EI+ Voltagm SIS 70S Soim»>46
333.9338 T:2 BSU3(256,30,-3.0) PKD(7,5,3,0.05\,184.0,1.00\rrrT) XxptXfCPS
TRIANGLE LABS Text:O-M23-3 TLI#43057 UKT. TIME "
1001 A4.48E7
23 > 09
80:
60:
40:
20:
o:
A2.58E
20:00 21:00
Tile:S975Bll #1-848 Acq:10-SEP-1997 23:06:56 EI+ Voltaya SIS 70S HOiu*:28
327.8847 T:2 BSOB(256,30, -3. 0) PB>(7,5,3,0.05\,112.0,1.00\rt,T) ErptSPCOS
TRIANGLE LABS Text:O-M23-3 TLH43057 UKT. TIME "
10 0\ A6.f8E7
80:
60:
40:
20:
o:
22OO
23:09
20:00 21:00
rilm:S975811 #1-848 Aeq:10-SEP-1997 23:06:56 EI+ Voltmya SIS 70S
330.9793 Ts2 Exp-.EPCVS
TRIANGLE LABS T»xt:O-M23-3 TLH43057 OKT. TIME - 2J;09
1001,
* „ 19>44 20:0620^22 30:41 20:58
80J 18'*S
60:
40.
20:
o:
I9\oo'
' 20\00~
21:00'
23:00'
-9.4E6
17.5X6
-.5.6X6
.3.8X6
-1.9X6
0.0X0
-1.1X7
.9.1X6
.6.8X6
.4. 6X6
-.3.316
,0.0X0
TiM*\
-1. 7X7
.1.3X7
'.1. 0X7
.6.7X6
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0.0X0
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.1.8X6
.8.8X5
0.0X0
177
-------
•110,5575811 #1-848 Acq:10-SEP-1997 23,06,56 El* Volttgt SIS 70S XoiMf,38
339.8597 Ts2 BSUB(256,30, -3.0) PKD(7,5,3,0.05\,152.0,l.OO\rr,T) XxptXPCUS
TRIANGLE LABS T*xt,O-M23-3 TLH43057 IKJ. TIMX - 23,09
1001 A2.35E5
23:00 24,00 25,00 ,
TlleiS975811 #1-848 AcqtlO-SEP-1997 23,06,56 XI* Volttgm SIS 70S moi*»:43
341.8567 r,2 BSVB(256,30,-3.0) PXD(7,5,3,O.OS\,172.0,1.00\,T,T) XxptXSCUS
TRIANGLE LABS TextiO-M23-3 TLH430S7 XKT. TIME!-
1001 A1.75JE5
23,00 24,00 25,00
rileiSS75811 #1-848 Acq: 10-SEP-19 97 23,06,56 EH- Volt*g» SIX 70S Boim»t37
351.9000 F:2 BSOB(256,30,-3.0) PKD(7,5,3,0.05\,148.0,1.00\,r,T) ErptXPCUS
TSIANSLE LABS Text:O-H23-3 TLH43057 HKT. TIKE
1001
26:00
23,09
80:
60:
40:
20:
23:00
25,00
26 tOO
23,09
.211X7
2600
rile:S975811 #1-848 Acqi 10-SEP-1997 33*06,56 SI+ Voltmgu SXS 70S m>imk,35
353.8970 T:2 BSOB(256,30t-3.0) PKD(7,5,3,0.05\r140.0,1.00\rf,T) XxptX^COS
TRIANGLE LABS Text:0-M23-3 TLH43A57
1003
80:
60:
40:
oJ
23:00 34,00 25*00
Fil»iS975811 #1-848 Acq:10-SEP-1997 23:06,56 XH- Valtmyu OX TVS
330.9792 Ts2 XxpiXPCUS
TSIANSLE LABS Text,O-H23-3 TLH43037 XKT. TTHE
100* 22,57 23:36 23,54 24:2O 24,41 24,51L, a5_i24
23,00 24,00 25,00
r±lo,S975811 #1-848 AcqilO-SEP-1997 23,06:56 XH- Voltmy* SIS 70S
409.7974 r,2 XxptXPCOS
TRIANGLE LABS T*zt:O-H23-3 TLHH39S7 JXT.
1001
26tOO
23,09
U..2X7
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.6.2X6
^3.1X6
9,0X0
-L.OXT
.t.4X6
.6.3X6
.4.2X6
'-.2.1X6
0.0X0
4.9X6
2J«00
24 00
25,00
2tfoO
17ft
-------
1
FiJ.es SS 7581 1 fJ-840 AcqtlO-SEP-1997 23t06t56 EI+ Voltage SIR 70S HoifetJS
355.8546 r,2 BSOB(256,30e -3.0) PKD(7,5,3,0.
TRIANGLE LABS TexttO-H23-3 1X1*43057
100]
80.
50.
40.
0
A1.62E5
I
OS\,152.0,1.00\,r,T) XzpiXPCOS
OKT. TIME - 23(09
A1.11E5 A1.22E5
|
A
1 \ I
1 \ " - - ' - - M^5»w
/ \A9.68X3 A1.32E4 ) A .
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24(00 ' 25(00
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25/00 Ti*e
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357.8516 Ti2 BSOB(256, 30, -3.0) PXD(7,5,3,0
TRIANGLE LABS Text:0-M23-3 1X1*43057
1003k A1.08X5
80.
50.
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A1.48£5 1
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24(00 ' ' ' 25,00
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ZMT. TIME • 23(09
-3.514
W£4
A2.84X4
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26 1 00 Time
r±le,S975811 41-848 Acq,10-SEP-1997 23(05(55 EH- Voltage SIS 70S Hoi*e,33
367.8949 Ti2 BSOB(256,30,-3.0) PKD(7,5,3,0
TRIANGLE LABS TextiO-H33-3 1X1*43057
1003
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40.
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24-00 ' 25(00
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0.0X0
25(00 ' ... ^^
ril«(S9 75811 fl-848 Aoq>10-SEP-1997 23(05(55 EH- Voltage SIS 70S Holme ,32
369.8919 F,2 BSVB(256,30, -3. 0) PKD(7,5,3,0
TRIANGLE LABS Text lO -If 23 -3 3X1*43057
100]
80.
50.
401
201
01
24(00 ' 25(00
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IKr. XIMX - 23(09
A2.00E7
K
I Ul.82£5
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26 tOO T±fe
r±le,S97S811 #1-848 Acq,10-SEP-1997 23(05(55 EH- Voltage SIS 70S
330.9792 r,2 ExpiEPCUS
TRIANGLE LABS Text,O-M23-3 TLH43057
100]
80.
60.
40.
20.
01
23,54 34,ao 24(41 2<«5'
v^^v 24 1 07 ^yv/wxvA /^"*A jJ*1*1**™
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24(00 25>00
UKT. TDtX - 23(09
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2tf(00 ... ;staB
179
-------
.Tile > 59 75811 #1-405 Acq:10-SEP-1997 23:06:56 EI+ Voltage SIR 70S KaiMm>1087
373.8208 Fi3 SSUS(256,30,-3.0) PKD(7, 5,3,0. 05\,4348. 0,1. 00\,F,T) XxftXfCOS •
TRIANGLE LASS T*xt:O-M23-3 XLH43057 HUT. TIME * 23,09
1001
80:
50:
40:
20:
A4 . 77X5
A3. 26X5 1/1 ;
11
A1.59£5ll / 1 A A1.99E5
Al \ A6.91E4 1 \rh.50E4 fA *
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27:24 27:3ff 27:48 28:00 28:12 28:24 28:35 28>48 29:00 29:12 29:24 29\36 a»:48 30:00 30:12
JX1*:5975811 #1-405 AcgjlO-SZP-1997 23,06,56 EI+ Voltagr» SIX 70S Ooltm,580
375.8178 F:3 SSUS(256, 30, -3.0) PXD(7,5,3,0.05\,2320.0,1.00\,T,T) XxptXPCUS
TRIANGLE LASS Tazt:O-M23-3 TLH43057 IX J. TIME - 23,09
1001
so:
50:
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•
A3.97E5
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" 27:24' 27:35' 27i48 28:00 ' 28*12' 28:24 2800 28:JL2 28\24 28:35 28148 29iOO 29:12 29:24 39i3f 1
7ila:5975811 #1-405 AoqtlO-SXt-1997 23,Of,Sf XI+ Voltfgm SIX 70S Ho±M»i955
385.8610 F,3 SSUS(256, 30, -3.0) PXD(7, 5, 3, 0.05^3820. 0,1. 00\,F,T) XxptXTCOS
TRIANGLE LASS Text:O-M23-3 TLH43OS7 OCT. XUO - 33,09
1001
80:
50:
40:
20:
0:
A3. 88X7
A3. 16X7 I
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A A
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27:24 27:J5 27:48 28»bi 28 tH 2J3«24 23 ,36 2*1^48 29:00 29,12 29:24 29*, 36 ;
Fil»iS975811 #1-405 Acq,10-SKP-19»7 23,08,56 XH- Volt»y» fix 70S
392.9760 F,3 XxpiXPCUS
TRIANGLE LASS TextsO-M23-3 XUI43057 IXT. TXHX - 2Jjfl9
14A1
;nn-
60-
401
20J
0:
?7f31 28,07 . 28,20 ^ j,
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445.7555 ft3 ExpiEPCUS
TRIANGLE LABS T»JCt,O-M23-3 HJ#4JC57 IJKT. TIME - 23:09
1003
80.
50.
40.
20.
0.
29>4<
27:52
29 1 12
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27:21 •27'I'1 3tt"\\
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180
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Fila:SS75Bll 11-405 AcqtlO-S£P-lS97 23:06:56 EI+ Voltage SIX
705 Noi*ett>J6
389.8156 F-,3 BSOB(256,30,-3.0) PXD(7,5,3,0.05\,2544.0,1.00\,r,T) ExpiEPCUS
TRIANGLE LABS Text:0-M23-3 TLH430S7 IKJ. TIME - 23s 09
1001
80.
601
40.
20.
A4.67E5
A
,
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^. ./v,
27:48 28:00 28:12 28\24 2B\ 36 2B\48 29\00
rile > 55 75011 1 1-4 05 AcqslO-StP-1997 23:06:56 Eli- Voltage SIX
A1.06E5
A A9.99E4
/A-- A,is«r r
_l.3S5
.1 . 0X5
-7. 7X4
-5.1X4
-2.6X4
29,12 29:24 29\36 29\4B Time
70S Noi»ei374
391.8127 T:3 SSUB(256,30,-3.0) PXD(7,5,3,0.05\,1496.0,l.OQ\rT,T) XzptXPCUS
TSIANGLE LABS Text:0-M23-3 TLH43057 INJ. TIME - 23:09
1001
80.
60.
40.
20.
A3. 4 8X5
A
I I A1.65K5
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27:48 28:00 ' 28:12 ' '28:24 ' 28t36 28:48 ' 29:00
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A7.57E4 A9.71X4
A iA
M/V ^^ / \__
-1.0X5
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29,12 ' 29\24 ' ' 29\36 '29,48 ' Tim*
70S Noise ,430
401.8558 F:3 BSUB(256, 30, -3.0) PXD(7,5r3rO.OS\r1720.0tl.QO\rT,T) XxptXPCUS
TSIANGLE LABS Text,O-H23-3 TLH43057 IXT. TIME - 23,09
1003
80.
60.
401
20.
0_
y
27:48 28:00 28:12 38:24 28:36 28\48 29\00
Tile:S975811 tl-405 Aoq:10-SXP-1997 23:06:56 EI+ Voltage SIX
A3. 12X7
*. A
f[f\
\ I I A1.23E7
A
A
1 A
V I V
7.0X6
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0 . 0X0
29,12 29\24 29:36 29t48 Tim*
70S HoiaetS66
403.8529 f:3 BSOB(256,30,-3.0) PXD(7,5,3,O.OS\,2264.0r1.00\,T,T) Elp,EPCU3
TSIANGLE LABS Text,O-M23-3 TLH430S7 IKT. TIME - 23:09
1001
80.
601
401
201
01
/
27:48 28:00 28:12 28:24 28:36 28\48 29\00
Tile, S97 5811 tl-405 AoqilO-SXP-1997 23:06:56 EH- Voltage SIX
392.9760 Ft3 Ezp:SPCUS
A1.74X7
\ l\
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A
A
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0 . 0X0
29:12 29:24 29:36 29:48 Time
70S
TSIANGLE LABS TeJct,0-M23-3 TU 443057 IJKT. TIME - 23:09
1001
80.
60.
401
201
0'-
37, CO 28i 07 28:20
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/v_,/^WVl'v\V\A/"''\ 28:3328i*t 28:51 •"£"*
>J^*' V*^W» ^ f\f^^^
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181
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407.7818 Ti4 SSUS(256,30, -3.0) PKD(7r5,3,0.05\t3180. 0,1.00\,r,T) ExpiKPCOS
TRIANGLE LABS TttIt:O-M23-3 TLH43057 TXT. TIMS - 23:09
1001 A3.85X5
BO:
eo:
31,12 31:24 31:36 31,48 32,00 32,12 32:24 32,36
rilm,S975811 tl-430 Acq,10-SXP-1997 23:06:56 XI* Voltfffo SIS 70S Boi*9t4l2
409.7789 T:4 BSUB(256,30,-3.0) PXD(7t5,3r0.05\r1648.0,1.00\,T,T) XxptXPCOS
TRIANGLE LABS Text,O-H23-3 TLIf43057 UKT. TIMS - 23,09
31tl2 31:24 31:36 31:48 32tOO 32:12 32:24 32:36
rile:S975ail tl-430 Acq>10-SXP-1997 23:06:56 EI+ VoZtaff* SIR 70S Noif*:522
417.8253 T:4 BSOB(256,30,-3.0) PXD(7,5,3,0.05\,2088.0,1.00\,T,T) ErptXPCUS
TRIANGLE LABS Text:O-M23-3 TLH43057 IJKT. TIMS ' 23:09
1001 A6.21E6
40:
OJ
A1.3SX5
A1.20E5
A1.90E4
32:48
100]
so:
40:
20:
A3.J3ES
A1.11XS
A7.35E4
4 A
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A1.45E4 /\
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32:48
so:
so:
40:
20:
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A4.18S6
31:12 31:24 31:36 31,48 32:00 32:12 32:24
ril*iS975811 tl-430 Acq:10-SEP-1997 23*96:56 ZT+ Valtmg* SIX 70S Bairn*1457
419.8220 F:4 BSOB(256,30t-3.0) PXD(7r5r3T0.a3\ria28.0,1.00\fT,T) XxpiSPCUS
TXIANGLX LABS Text:O-H23-3 TOH43AS7 XfJ. ZHB * 23.109
1001 A1.46E7
32i36
32148
80:
60:
40:
20:
o.
A1.04Z7
31:12 31:24 31t36 31,48
r±le:S975Sll tl-430 Ac?,10-SEP-1997 23tOf*M ZT+
430.9729 Ti4 ExpiEPCUS
TRIANGLE LABS T
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nie,S975Bll tl-430 Ac4 BSOB(256,30,-3.0) PXD(7,5,3,Q.05\,112.0,1.00\,T,T) XxpiEPCUS
TSIANSLE LABS TextsO-M23-3 TLII430S7 1WT. TIME • 23,09
1004
80.
60.
40.
20.
0.
3
Al . SJE5
A1.24S5 1 \
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1:18 31:24 31:30 31:35 31:42 31:48 31:54 32>00' 37:06 32:12 32:18 32^24 32,30
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rileiS975811 tl-430 Acq, 10 -SEP -19 97 23,06,56 EH- Voltage SIX 70S Xoi»e,31
425.7737 ri4 BSUB.(256,30,-3.0) PXD(7,5,3,0.05\,124.0,1.00\,F,T) ExpiEPCOS
TRIANGLE LABS Text,O-H23-3 TLIt43057 INJ. TIME - 23,09
1003
80.
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40.
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0.
A1.59E5 A1.70E5
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31:18 31:24 31:30 31 1 3(5 31:42' 31:48 31:54 32:00 '32:06 32:12 32:18 32:24' 32:30
r5.4X4
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Mle i SS 75811 tl-430 AcqtlO-SEP-1997 23*06 1 56 XI* Voltage SIX 70S lfoiae,709
435.8169 r>4 BSUB(256,30,-3.0) PXJ>( 7,5,3, 0.051,2836. 0,1. 00\,r,T) ExptXPCOS
TXIASSLE LABS Tejtt>O-M23-3 TLXt43057 HUT. TIME • 23,09
1001
80J
60.
40.
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Exp : EPCUS
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Sample Text:0-M23-3 TLI#43057 INJ. TIME - 23:09 File Text:O-M23-3 TLI#4»
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TLI Project: 43057
Client Sample: O-M23-3
Method 23 TCDD/TCDF Analysis (DB-225)
Analysis File: P973846
Client Project:
Sample Matrix:
TLI ID:
Sample Size:
Dry Weight
GC Column:
M23TRAIN
181-27-4A-C
1.000
n/a
DB-225
Date Received:
Date Extracted:
Date Analyzed:
Dilution Factor
Blank File:
Analyst
08/29/97
09/06/97
09/12/97
n/a
S975807
WK
Spike File:
ICaL
ConCaU
% Moisture:
%Lipid:
% Solids:
SPC2NF04
PF22206
P973843
n/a
n/a
n/a
«C,j-l,2,3,4-TCDD
0.02
0.85
20:42
B_
0.80
19:44
Data Reviewer.
lofl
Triangle Laboratories, Inc.®
801 Capitola Drive • Durham, North Carolina 27713
Phone: (919) 544-5729 - Fax: (919) 544-5491
09/12/97
ONFJSK vUOO. LAKS 6.WM
Printed: 14:57 09/12/97
194
-------
Initial
Date..
Data Review By:
Calculated Noise Area: n/a
The Total Area for each peak with an ion abundance ratio outaide
ratio limits has been recalculated according to method requirement*.
Page No.
09/12/97
Listing of P973846B.dbf
Matched GC Peaks / Ratio / Bet. Time
Compound/
M_Z QC.Log Omit Why ..RT. OK Ratio Total.Area... Area.Peak.1..
TCDF
304-306
MK
304-306
13C12-TCDF
316-318
316-318
13C12-TCDD
332-334
332-334
DC
DC
DC
DC
DC
DC
DC
DC
DC
DC
DC
DC
DC
DC
DC
DC
DC
DC
NL<
SN
SN
SN
SN
SN
SN
SN
1
NL
WL
SN
SN
WH
1
NL
SN
SN
HH
WH
2
0:00
17:17
18:15
19:00
19:26
20:42
21:09
21:26
22:30
Peak
0:00
19:24
20:40
21:13
21:37
22:31
Peak
0:00
18:26
19:29
19:44
20:23
21:30
21:56
Peaks
0.
RO
RO
RO
RO
RO
0.
RO
RO
RO
0.
RO
RO
RO
65-0.89
0.72
0.58
1.06
0.34
0.77
0.85
0.71
0.92
0.57
65-0.89
0.99
0.85
0.77
0.73
2.39
0.48
65-0.89
1.37
0.74
0.79
0.80
0.81
0.60
0.94
2.68
4.85
0.62
1.33
10.77
13.00 5.98
1.92
0.69
1.56
13.00
2.46
15.86
3,307.74 1,434.55
9.13
5.42
16.64
3,307.74
Above: TCDF / TCDD Follows •
Area.Peak.2.. Rel.RT Compound.Nome.. ID.. Flag*.
0.786-1.096
0.000
0.836
0.883
0.919
0.940
7.02 1.002 2378-TCDF AN
1.023
1.037
1.089
0.952-1.048
0.000
0.939
1,873.19 1.000 13C12-2378-TCDF ISO
1.027
1.046
1.090
2.25
12.45
2,580.19
1,612.66
34.52
1.70
16.37
4,192.85
0.897-1.103
0.000
0.946
1,
135
717
.41
.25
1,444
895
.78
.41
1
1
1
1
1
.000
.013
.046
.104
.126
13C12-2378-TCDD
13C12-1234-TCDD
IS1
RSI
Column Description 'Why* Code Description QC Log Deso,
M_Z -Nominal Ion Nasa(es)
..RT. -Retention Time (mm:as)
Rat.l -Ratio of M/M+2 Ions
OK -RO-Ratio outside Limits
Rel.RT-Relative Retention Time
••• End of Report •••
WL-Below Retention Time Window
HH-Above Retention Time Window
SN-Below Signal to Noise Level
-------
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TRIANGLE LABS TtacttO-H23-3 TLIf 43057
100* A4.69X4 AS. 70X4
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rll*iP973846 fl-755 Acqil2-8XP-1997 13t32ilO XH- Voltag* 5X8 70P Ho±f»i688
315.9419 BSU3(2S6,30,-3.0) TXD(5t3,lf0.10\,2752<0,0.00\,T,T) XxptDB235
TSIJUfGLE LASS Text:0-M23-3 TLH43057
1001 A1.13X7
801
601
401
201
22100
01
17100 18,0* X*iM 30100 21*00
r±l»tP973846 fl-755 Acxj112-SXP-1997 13t32tlO XI+ Volttg* SIX 70P OOimmi696
317.9389 BSUB(256,30,-3.0) PXD(5,3,l,0.10\,2784.0,0.00*,r,r) Elp>DB32S
TJtlASGLX LABS T*xtiO-M33-3 TLH43057
1001 A1.97X7
801
601
40.
30.
32 tOO
17100 10)00 15.00 30100
r±l»tP973846 fl-755 Acq,12-SXP-1997 13t32tlO XH- Voltmgm SIS 70P
375.8364 XxpiDB225
TRIANGLX LABS T*XttO-M23-3 9ZTMM57
100115*27
80.
60.
21100
22100
40.
20.
0.
18,33
18,01
19130
30,25 30,58 21i38 31,54 23,21
2.2X4
-3.7X6
J.QX6
-2..2X6
-L.5JW
.7.4X5
0.0X0
TlMtfi
-4.9X6
-3.9X6
-3.9X6
.3.0X6
.9.8X5
0.0X0
.7.3X4
.5.5X4
.3.6X4
.1. 8X4
0.0X0
17 tOO
18,00
19,00
30,00
21 > 00
23,00
196
-------
FilatPS/3846 #1-755 Acq:JLi-SEP-lS97 13l32tiQ EH- Voltaya SIS 7OP KD1M9
319.8965 BSVB(256,30,-3.0) PXD(5,3,l,0.10\,2252.0,0.00\,r,r) CxpiDB225
TRIANGLE LASS Taxt:0-M23-3 TLH43057
100* A2.01E4
18*00 19100 20*00 21100
T±l9tP973S46 #1-755 Acq,12-SEP-1997 13t32ilO EH- Voltage SIX 70P Hoimmi627
321.8936 BSUB(256t30,-3.0) PKD(5,3,lr0.10\,2S08.0rO.OO\,TrT) SxpiDB225
TRIANGLE LABS T*xttO-M23-3 TLH43057
100* A3.50X4
ISiOO 19:00 20 tOO 2l'iOO
FiletP973B46 #1-755 Acq>12-SEP-1997 13i32tlO EI+ Voltmym SIS 70T Soif*i509
327.8847 BSUB(256,30,-3.0) PKD<5,3,l,0.10\,3036.0,0.00\,rrT) Exp>DB225
TSIAHSLX LABS T*rtiO-M23-3 XLIt43057
1001
eo:
SO.
40.
20:
o:
A2.14X7
18.00 15«00 20iOO 21tOO
ril»tP973846 #1-755 Acq>12-SEP-1997 13i32>10 SI+ Voltmg* SIX 70P Hoi*ut870
331.9368 BSOB(2S6,30,-3.0) PKD(S,3,l,0.10\,3480.0,0.00\,r,r) 3SxptDB225
TSIAJTSLS LABS T»XtiO-H23-3 TLH43057
1004 A1.14S7
so:
so:
40.
20.
18*00 19t00 20i00 ailOO
Til»tP973846 #1-755 Aoqtl2-SfP-1997 13t32ilO EH- Volt*y* SIX 7OP Koi»»i636
333.9338 BSUB(256,30,-3.0) PKD(5,3,lt0.10\,2S44.0,0.00\,T,T) XzpiDB225
TRIANGLE LABS T»xttO-M23-3 TLH43057
100\ A1.44X7
80.
60.
40.
20:
0.
8.95X6
18100
is!00'
20100
21\QO
22100
23 tOO
22100
22,00
-5.3XS
.4.3X6
.3.2X6
J.1X6
.1.1X6
0.0X0
Ximm
.3.4X6
.1.8X6
.1.2X6
.6.0X5
0.0X0
-3.7X6
.3.0X6
.2.2X6
J..SX6
.7.4X5
22*00
.0.0X0
KLmu
197
-------
ril«,P913846 #1-755 Acxjtl2-SEP-1997 13,33,10 JBT+
303.9016 Exp,DB335
TRIANGLE LABS T*xt,0-H23-3 TLH43057
19136
17>00 18,00 19,00 20,00 21,00
ril»,P973846 11-755 Acqtl3-SXP-1997 13*33tlO XX+ Voltage SIM 7OP
315.9419 Exp,DB325
TXIAMGLX LABS T*xttO-M33-3 TLIH3957
1003, 30\40
80.
SO.
40:
20:
ol
23,00
17,00 18,00 19,00
Fil»,P973846 tl-755 Acgtl2-SXP-1997 13133tit
319.8965 XxptDB335
TBIANGLS LABS T9XttO-H23-3 TLlt43057
1003\
I7iia
804 Jl *7>*9
18,38
60:
40:
20:
ol
30,00
1+ VUtag
ait oo
'aaioo
70P
17.00 18.00 I9i«t
ril(nP973846 H-755 Acqil3-SXP-1997 13>33,19 JBT-f
331.9368 ExpiDBaaS
LABS T*xtiO-M23-3 -01943057
ai to
33t»0
TOP
1003
80:
60:
40:
20:
ol
17,00 18:00 19,00 20,00
Til*,P973846 tl-755 Aoqtia-SXP-1997 13,33,19 XI+ VtaU^i
292.9825 Eip,DB235
XXXAHGLX LABS Ttuct.,O-M23-3 TLH43057
18,39 It 131 19t4t
ait oo
70P
lOOi
80:
eo:
40:
20:
17,00 17s30
22,00
21*57
17,00 18,00 19,00
ril»,P973846 tl-755 Acq,12-SKP-l»97 13t32tlO XX+ Voltxym SIX 70P
330.9792 SxptDB235
TXIAHSLX LABS Toxt,0-M33-3 TLTt43057
17tOO 17,32
x*v ^+.
80:
60:
40:
20:
o.
32 tOO
-3.7X6
.3.0X6
.3.2X6
.1.5X6
.7.5X5
.O.OXO
3. OX*
i.
LI.J
.6.0X5
.0.0X0
T±mt
^8.3X6
-.6.6X6
.4.9X6
.3.3X6
-1.6X6
0.0X0
33,41
17,00
18.00
,9.2X6
1.7.3X6
.3.5X6
.3.7X6
.1.8X6
0.0X0
15.00
22100
198
-------
fl:P973846
Ref. aass 292,3825 Peak top
Height 1,92 volts Span 288 pc*
Systei file naie
Data file naie
Resolution
Group nuaber
lonlzatlon lode
Suitchlng
Ref, lasses 292.3825,
R 232,3885
6 383,9816
C 385.8987
D 315,3419
E 317.9389
F 319.8965
6 321,8936
H 327,8847
I 338.9792
J
K
L
M
1
El*
VOLTRGE
388.9761
338.9792
331.9368
333.9338
375.8384
Channel I 338.9792 Peak top
Helpj* 1.94 volts Span 288 ppe
199
-------
200
-------
TLI Project: 43057
Client Sample: O-M23-FB
Method 23 PCDD/PCDF Analysis (a)
Analysis File: S975816
Client Project*
Sample Matrix:
TLI ID:
Sample Size:
Dry Weight
GC Column:
M23TRAIN
181-27-5A-C
1.000
n/a
DB-5
Date Received:
Date Extracted:
Date Analyzed:
Dilution Factor
Blank File:
Analyst:
08/29/97
09/06/97
09/11/97
n/a
S975807
HLM
Spike File:
ICal:
ConCal:
% Moisture:
% Lipid:
% Solids:
SPX23704
SF56117
S975814
n/a
n/a
n/a
£aalp£^;'vif%
2,3,7,8-TCDD
1,2,3,7,8-PeCDD
1,2^,4,7,8-HxCDD
1,2,3,6,7,8-HxCDD
1,2,3,7,8,9-HxCDD
1,23,4,6,7,8-HpCDD
1,2^,4,6,7,8,9-OCDD
2,3,7,8-TCDF
1,23,7,8-PeCDF
2,3,4,7,8-PeCDF
1,23,4,7,8-HxCDF
1,2^,6,7,8-HxCDF
2,3,4,6,7,8-HxCDF
1,2,3,7,8,9-HxCDF
1,2,3,4,6,7,8-HpCDF
1,2^,4,7,8,9-HpCDF
1,2^,4,6,7,8,9-OCDF
jotaW- jr^"^^
Total TCDD
Total PeCDD
Total HxCDD
Total HpCDD
Total TCDF
Total PeCDF
Total HxCDF
Total HpCDF
^^,«if^|
ND
ND
ND
EMPC
EMPC
0.06
0.11
ND
EMPC
0.03
0.07
0.03
0.03
ND
EMPC
0.04
0.07
;v^'?|»Bt''t4j
EMPC
0.02
0.06
0.06
ND
0.03
0.13
0.10
0.01
0.01
0.01
0.02
0.02
1.02 32:03
0.86 34:33
0.006
0.01
1.49 25:28
1.43 28:21
1.10 28:28
1.21 28:59
0.01
0.09
1.02 32:24
0.88 34:39
0.02
1 0.07
1 0.13
1 0.11
0.006
1 0.04
3 0.18
3 0.18
PR.
B_
B_
B
B_
B
PRB
PRB
B_
B_
Page 1 of2
X237_FS» lUO. LU31 ttO»
Triangle Laboratories, Inc.®
801 Capitola Drive • Durham. North Carolina 27713
Phone: (919) 544-5729 • Fax: (919) 544-5491
Printed: 1458 09/11/37
201
-------
TLI Project: 43057
Client Sample: O-M23-FB
Method 23 PCDD/PCDF Analysis (a)
Analysis File: S975816
!JCi2-2^,7,8-TCDF
l3C,r2,3,7,8-TCDD
13C,j-lA3,7,8-PeCDF
13Cn-lA3,7,8-PeCDD
l3C,rlA3,6,7,8-HxCDF
>3CB-lA3,6,7,8-HxCDD
»3Cu-lA3,4,6,7,8-HpCDF
"C,2-1A3,4,6,7,8,9-OCT>D
2.0
1.4
1.8
2.2
1.4
1.6
1.3
1.5
3.0
49.5
34.3
44.9
54.8
34.7
40.1
32.7
38.2
36.9
40%-130%
40%-130%
40%-130%
40%-130%
40%-130%
40%-130%
25%-130%
25%-130%
25%-130%
0.75
0.80
1.65
1.45
0.48
1.14
0.42
0.98
0.81
20:22
21:11
24:42
25:50
28:28
29:11
31:10
32.-02
34:32
J7CU-23,7,8-TCDD
13Ci2-2^,4,7,8-PeCDF
l3Cu-lA3,4,7,8-HxCDF
" \~-*r^- f -f^^ -j?* T fy&?
4.9
4^
f 3.6
) 33
)F 3.4
ssf5"''^'^ {"**&«. i r ff .
123
112
91.1
82.4
85.4
70%-140%
70%-140%
70%-140%
70%-140%
70%-140%
1.49
0.48
1.24
0.43
21:13
25:27
28:21
29^)6
77^77.
.
—
13Co-lA3,7,8,9-HxCDF
13Cir-2^,4,6,7,8-HxCDF
13C,2-1A3,4-TCDD
'3Cl2-lA3.7,8,9-HxCDD
0.86
1.18
20-.58
29:28
Data Reviewer
Triangle Laboratories, Inc.®
801 Capitola Drive • Durham, North Carolina 27713
Phone: (919) 544-5729 • Fax: (919) 544-5491
09/11/97
Page 2 of2
Printed: 14:58 09/11/97
202
-------
In
'
itial
Data Review By:
fc T
Calculated Noise Area:
1.67
The Total Area for each peak with an ion abundance ratio outside
ratio limits has been recalculated according to Method requirements.
Page No.
09/11/97
Listing of S975816B.dbf
Matched GC Peaks / Ratio /
Ret. Time
Compound/
M_Z QC.Log Omit Why ..RT. OK Ratio Total.Area... Area.Peak.1.. Area.Peak.2.. Rel.RT Compound.
ID.. Flags.
TCDF
304-306
D
304-306
13C12-TCDF
316-318
316-318
TCDD
320-322
320-322
DC
DC
DC
DC
DC
DC
D
DC
DC
DC
DC
DC
DC
DC
DC
DC
DC
DC
DC
DC
DC
DC
DC
DC
DC
DC
DC
DC
DC
DC
NL
SN
SN
SN
SN
SN
SN
SN
0
NL
ML
WL
NL
SN
WH
WH
2
NL
SN
SN
SN
SN
SN
SN
SN
SN
SN
SN
SN
SN
SN
SN
1
0:00
16:53
17:47
18:44
19:11
19:53
20:24
21:54
Peaks
0:00
18:02
19:10
19:20
19:30
19:51
20:22
21:41
22:40
Peaks
0:00
18:16
18:27
18:55
19:03
19:22
19:39
19:52
20:07
20:37
20:51
21:12
21:36
21:58
22:07
22:09
Peak
0.
RO
RO
RO
RO
RO
0.
RO
RO
RO
RO
RO
RO
0.
RO
RO
RO
RO
RO
65-0.89
0.
0.
0.
1.
1.
0.
0.
0.
67
63
46
58
03
55
77
65
1.
1.
0.
1.
3.
3.
6.
2.
0.
12
59
83
38
65
03
03
58
00
65-0.89
0.
0.
0.
0.
0.
0.
0.
1.
0.
14
23
58
58
69
76
75 2,
36
94
2,
65-0.89
5.25
0.90
0.36
0.23
0.91
0.66
RO
RO
RO
RO
RO
RO
RO
RO
RO
RO
3.07
0.57
1.95
0.98
0.
.59
0.33
0.50
0.52
1,
.16
1.98
0.
1.
7.
2.
3.
12.
231.
3.
3.
16
06
36
41
05
39 5.36
29 953 . 97
03
82
0.820-1.101
0.
0.
0.
0.
0.
0.
1.
1.
0.951-
0.
0.
0.
0.
0.
7.03 0.
1,277.32 1.
1.
000
829
873
920
942
976
002 2378 -TCDF AN
075
1.049
000
885
941
949
957
975
000 13C12-2378-TCDF ISO
065
1.113
243.68
0.
5.
0.
0.
2.
14
93 3.02
62
32
12
1.11
0.
50
1.93
1.12
1.06
0.39
1.75
1.
,40
0.90
0.34
0.99
0.853-1.059
0.000
3.35 0.862
0.
,871
0.893
0.899
0.914
0.928
0.938
0.950
0.973
0
.984
1.001 2378 -TCDD AN
1.020
1.037
1
1
.044
.046
5.93
Triangle Laboratories, Inc.® Analytical Services Division
801 Capitals Drive • Durham, North Carolina 27713
Phone: (919) 544-5729 • Fax: (919) 544-5491
Printed: 14:58 09/11/97
203
-------
Page Ho. 2
09/11/97
Compound/
H_Z QC.Log Omit Why
Lifting of S975816B.dbf
Matched GC Peaks / Ratio / Ret.
. RT. OK Ratio Total. Area. .. Urtm Pealr.l. . Area. Peak. 2. . Rel.BX Co*paaad.]
TT»
37C1-TCDD
328
328
13C12-TCDD
332-334
332-334
P«COF
340-342
M
D
340-3(2
13C12-PeCDF
352-354
DC
DC
DC
DC
DC
DC
DC
DC
DC
DC
DC
DC
DC
DC
DC
DC
DC
DC
DC
DC
DC
D
DC
DC
DC
DC
DC
DC
DC
DC
NL
HL
HL
HL
SN
SN
SN
SN
SN
SN
SN
SN
SN
3
NL
4
NL
SN
SN
SN
SN
SN
SN
SN
SN
SN
SN
SN
SN
WH
WH
2
NL
0:00
18:08
18:35
18:44
19:39
20:14
20:55
21:13
21:27
21:32
21:41
21:48
22:05
22:12
22:31
22:44
Peaks
0:00
19:52
20:58
21:11
21:35
Peaks
0:00
22:35
22:42
23:11
23:58
24:11
24:42
24:53
25:02
25:15
25:28
25:37
25:55
26:15
26 : 28
26:50
27:00
Peaks
0:00
23:48
0.
RO
RO
RO
1.
RO
RO
RO
RO
RO
RO
RO
RO
RO
RO
RO
RO
RO
RO
RO
RO
1.
RO
1
1
0.
0.
2.
2.
70.
0.
0.
,299.
1.
1.
2.
1.
1.
0.
1.
1.
,372.
09
75
67
10
71 70.71
59
84
45 1,299.45
92
97
23 2.23
30
38
90
27
21
39
65-0.89
22
0
0
0
1
.13
.90
.86 3
.80 1
.06
4
32-1.78
0
0
0
0
1
10
0
1
1
0
1
1
3
3
0
0
1
.16
.93
.24
.36
.87
.79
.95
.10
.15
.25
.49
.95
.02
.90
.77
.70
.15
0.
6.
,420.
,251.
22.
14
97 3.53
S3 1,590.25
49 555.65
05 13.26
0.906-1.094
0.000
0.856
0.877
0.884
0.928
0.955
0.987
1.002 37C1-TCDD
1.013
1.017
1.024
1.029
1.042
1.048
1.063
1.073
yT**t
0.906-1.094
0.
3.94 0.
1,640.28 0.
695.84 1.
12.46 1.
000
938
990 13C12.-1234-TCDD
000 13CL2-23.78-TCDD
019
RSI
IS1
,701.04 •
TODU / PtCDF XtfcUeira --
0.
2.
0.
0.
2.
0.
5.
3.
5.
0.
14.
5.
1.
1.
2.
1.
1.
19.
iO
as
41
72
40
48
45 3.31
47
35
72
41 t.62
10
43
22
37
66
55
86
32-1.78
0
1
.88
.51
0.
I.
12
61 S.78
0.907-1.078
0.
0.
0.
0.
0.
0.
3.49 1.
1.
1.
1.
5.79 1.
1.
1.
1.
1.
1.
1.
000
914
919
939
970
979
000 12378-PeCDF
007
013
022
031 23478 -PeCDF
037
049
063
072
086
093
AN
AN
0.436-1.162
0.
3. 83 0.
000
964
Triangle Laboratories, Inc.® Analytical Services DMston
801 Capitola Drive • Durham, North Carolina 27713
Phone: (919) 544-5729 • Fax: (919) 544-5491
Printed: 14:58 09/11/97
2Q4
-------
ige No.
Listing of S975816B.dbf
Matched GC Peaks / Ratio / Ret. Time
impound/
_Z.... QC.Log Omit Why ..RT. OK Ratio Total.Area.
Area.Peak.1. . Area.Peak.2.. Rel.RT Compound.Name.. ID.. Flags.
52-354
sCDD
56-358
56-358
5C12-PeCDD
58-370
58-370
tCDF
'4-376
DC
DC
DC
DC
DC
DC
DC
DC
DC
DC
DC
DC
DC
DC
SM
SN
7
NL
SN
SN
SN
SN
SN
SN
SN
WH
3
NL
SN
SN
24:
24:
24:
25:
25:
25:
25:
26:
20
42
53
00
27
44
51
28
RO
RO
RO
RO
1.
1.
1.
1.
1.
2.
1.
0.
Peaks
0:
23:
24:
24:
24:
25:
25:
25:
25:
25:
26:
00
58
27
44
50
04
17
31
50
59
10
26:40
1.
RO
RO
RO
RO
RO
RO
RO
RO
RO
RO
32-
13.
0.
7.
1.
3.
1.
1.
3.
2.
3.
0.
38
65
81
55
49
86
16
92
1.78
80
31
11
36
34
23
62
38
49
11
88
1.01
Peaks
0:00
24:13
25:03
1.
RO
RO
RO
25:50
DC
DC
DC
DC
DC
D
DC
D
D
SN
SN
SN
2
NL
SN
SN
SN
SN
SN
25:
:59
26:08
26:
26:
:14
:23
6.
1,740.
12.
13.
1,897.
3.
3.
5.
69 3.88
67 1,084.59
93 9.18
81 8.39
18 1,135.82
75
04
71 3.47
2.81 0.
656.08 1.
5.07 1.
5.42 1.
761.36 1.
1.
1.
3.79 1.
985
000 13C12-PeCDF 123
007
012
030 13C12-PeCDF 234
042
047
072
IS2
SOR2
3,686.60
0.
9.
0.
8.
0.
6.
2.
13
94 6.04
46
65 4.98
97
27 3.81
80
2.70
4.
82
0.94
0.
86
1.45
0.921-1.026
0.
19.68 0.
0.
3.67 0.
0.
3.09 0.
0.
0.
1.
1.
000
928
946
957
961
970
979
988
000 12378-PeCDD
006
AN
1.013
1.032
24.86
32-1.78
1.
,29
1.95
0.62
1.45
1.58
RO
RO
RO
0.93
3.75
2.91
Peaks
0
27
27
27
27
27
28
28
28
28
28
:00
:21
:32
:40
:49
:58
:21
:28
:34
:47
:59
1.
RO
RO
RO
RO
RO
,05-1.43
1.86
1
1
1
1
1
1
1
1
0
1
.48
.46
.04
.31
.32
.43
.10
.18
.79
.21
0
.15
1.50
1,
1,189
119
1
0
1
.63
.98 703.40
.39 73.12
.74
.61
.38
0.845-1.155
0.
,000
0.937
0.970
486.58 1.000 13C12-PeCDD 123
46.27 1.
.006
IS3
1.012
1.015
1.
.021
1,309.37
1
8
18
1
5
4
32
15
4
4
16
.57
.49 5.60
.66 12.19
.73
.06
.36
.67 19.24
.58 8.16
.65
.17
.81 9.22
0.955-1.052
0
.000
3.79 0.961
8.33 0
0
0
0
13.43 0
7.42 1
1
1
7.59 1
.967
.972
.977
.982
.996 123478-HxCDF
.000 123678-HXCDF
.004
.011
.018 234678-HxCDF
AN
AN
AN
PR
iangle Laboratories, Inc.® Analytical Services Division
1 Capitola Drive • Durham, North Carolina 27713
icne: (919) 544-5729 • Fax: (919) 544-5491
Printed: 14:58 09/11/97
203
-------
Page No. 4
09/11/97
Compound/
M_Z.... QC.Log Omit Why
Listing of S97S816B.dbf
Matched GC Peaks / Ratio / Ret. Tiae
.RT. OK Ratio Total.Area... Area.Peak.1. . Area.Peak.2.. Rel.RT Compound.Kane.. ID.. Flags.
D
0
374-376
13C12-HXCDF
384-386
384-386
HxCDD
390-392
D
H
M
390-392
13C12-HXCDD
402-404
DC
DC
DC
DC
D
D
DC
DC
DC
DC
DC
DC
DC
DC
DC
DC
DC
DC
D
DC
DC
DC
DC
DC
DC
DC
DC
DC
DC
DC
DC
SN
SN
SN
SN
SN
SN
HH
WH
WH
5
NL
SN
SN
SN
SN
SN
SN
SN
4
NL
SN
SN
SN
SN
SN
SN
SN
SN
SN
SN
SN
WH
4
NL
29:
10
29:23
29:
29:
29:
29:
30:
30:
30:
29
33
41
46
02
05
09
RO
RO
RO
RO
RO
RO
RO
1
6
3
3
1
1
2
0
2
.14
.40
.24
.42
.24
.56
.87
.70
.30
Peaks
0:
27:
28:
28:
28:
28:
28:
29:
29:
29:
29:
30:
00
30
21
28
43
50
58
10
41
54
58
08
0.
RO
RO
RO
RO
RO
RO
RO
1.
0.
0.
0.
6.
4.
0.
0.
0.
92.
39
67
47
27
64
88
67
47
60
21
43-0.59
0
0
0
0
0
0
0
1
0
1
2
0
Peaks
0:
27:
28:
28:
28:
28:
28:
28:
28:
28:
28:
28:
29:
29:
29:
29:
29:
00
55
00
03
08
15
21
26
35
43
51
54
06
11
20
29
57
1.
RO
RO
RO
RO
RO
RO
RO
RO
RO
RO
RO
RO
RO
.37
.41
.48
.48
.94
.38
.49
.35
.49
.00
.07
.58
05-1.43
0
1
0
1
0
0
1
1
0
2
0
0
0
1
0
0
3
.63
.06
.38
.37
.66
.23
.26
.16
.97
.02
.77
.38
.62
.48
.06
.95
.29
Peaks
0:
28:
29:
00
35
06
1.
RO
2.
4.
1,360.
1,558.
2.
1.
1,420.
1.
1,164.
2.
1.
2.
78
91
71
16
22
69
56
65
20
49
56
27
5,503.63
: HxCDF / teC
0.
4.
0.
0.
0.
0.
24.
2.
10.
1.
0.
0.
2.
7.
0.
8.
0.
50.
65
81
45
45
52
27
46
03
06
01
36
70
85
53
07
13
63
18
05-1.43
0
1
1
.52
.35
.24
0.
5.
1,192.
79
64
66
1
1
1
1
1
1
1
1
1
.025
.032
.036
.038
.043 123789 -HxCDF AN
.046
.055
.057
.059
0.859-1.141
0
0
441.73 918.98 0
506.87 1,051.29 1
1
1
4 67-. 71 952.85 1
1
383.10 781.10 1
1
a
.000
.966
.996 13C12-HXCDF 478 SDR3
.000 13C12-BXCDF 678 IS4
.009
.013
.018 13C12- HxCDF 234 ALT 2
.025
.043 13C12-HXCDF 789 MJ1
.050
.053
1.059
0.950-1.015
0
0
0
0
0
0
13.65 10.81 0
0
5.57 5.76 0
0
0
0
0
4.97 3.36 1
1
4.50 4.74 1
1
.000
.957
.959
.961
.964
.968
.971
.974
.979
.984
.989
.990
.997 123478-HxCDD AN
.000 123 678 -HxCDD AN
.005
.010 123789-HxCDD AN PR
.026
0.966-1.034
0
3.36 2.48 0
659.69 532.97 0
.000
.979
.997 13C12- HxCDD 478 SUR4
Triangle Laboratories, Inc.® Analytical Services Division
801 Capitola Drive • Durham, North Carolina 27713
Phone: (919) 544-5729 • Fax: (919) 544-5491
Printed: 14:58 09/11/97
206
-------
ge No.
/11/97
Listing of S975816B.dbf
Matched GC Peaks / Ratio / Ret.
Time
npound/
Z.... QC.Log Omit why ..RT. OK Ratio Total.Area. .. Area.Peak.1.. Area.Peak.2.. Rel.RT Compound.Name.. ID.. Flags.
2-404
CDF
8-410
8-410
C12-HpCDF
8-420
8-420
COD
4-426
4-426
SI2-HpCDD
6-438
5-438
3F
2-444
DC
DC
DC
DC
DC
DC
DC
DC
DC
DC
DC
DC
DC
DC
DC
DC
DC
DC
DC
DC
SN
4
NL
SN
WH
4
NL
SN
SN
SN
2
NL
SN
SN
2
NL
1
NL
SN
SN
SN
SN
SN
SN
SN
29:
29:
29:
11
28
43
RO
1.
1.
0.
Peaks
0:
31:
31:
31:
32:
32:
32:
00
11
24
31
08
24
39
0.
RO
RO
14
18
63
- - - - ADOVB :
88-1.20
2.52
1.32
1,
.14
1.00
RO
RO
3
1,
3
.45
.02
.94
Peaks
0:
31:
32:
32:
32:
32:
00
10
02
22
39
48
0.
RO
RO
1,488.
3,734.
3.
29 794.20
26 2,022.59
74
694.09 1.
1,711.67 1.
1.
000 13C12-HXCDD 678
010 13C12-HXCDD 789
018
ISS
RS2
6,421.05
0.
35.
10.
10.
0.
13.
0.
69.
67
70 23.10
15 5.41
97 5.48
45
14 6.62
71
96
37-0.51
1.42
0
0
.42
.83
0.43
RO
1
.71
0.47
Peaks
0:
31:
31:
31:
32:
00
17
26
51
03
0.
RO
RO
RO
RO
88-1.20
0
0
1
3
1
.81
.32
.29
.44
.02
Peaks
0:
32:
00
02
0.
0.
1,082.
1.
712.
1.
2.
96
87 322.74
41
92 212.82
68
77
0.995-1.044
0.
17.50 1.
4.74 1.
5.49 1.
1.
6.52 1.
1.
000
001 1234678-HpCDF
007
Oil
031
040 1234789-HpCDF
048
AN
AN
0.936-1.128
0.
000
760.13 1.000 13C12-HpCDF 678
1.
500.10 1.
028
039 13C12- HpCDF 789
IS6
SUR5
1.048
1.052
1,795.79
: HpCDF / HpCDD Follows * ~~
0.69
0.57
13.
.16 8.29
0.51
20.03 10.10
0.976-1.006
0.000
0,
.977
6.45 0.981
0
.994
9.93 1.001 1234678-HpCDD
AN
33.19
88-1.20
1
0
Peak
0:
00
30:55
31:13
31:17
31:29
31;
;48
32:16
0.
RO
RO
RO
RO
RO
RO
32:25
76
1
0
0
3
1
1
2
1
.00
.98
-1.02
.00
.22
.22
.50
.63
.89
.46
.00
3,
1,162
.24
.82 574.07
1,162.82
: HpCDD / Octa~CDD &nd CDF
0
0
0
0
1
1
.12
.47
.68
.45
.17
.02
1.30
0
.84
0.969-1.031
0
588.75 1
.000
.000 13012-HpCDD 678
IS7
0.884-1.116
0
0
0
0
0
0
0
0
.000
.895
.904
.906
.912
.921
.934
.939
PR
angle Laboratories, Inc.® Analytical Services Division
Capitola Drive • Durham, North Carolina 27713
)ne: (919) 544-5729 • Fax: (919) 544-5491
Printed: 14:58 09/11/97
207
-------
Page No. 6 Listing of S975816B.dbf
09/11/97 Matched GC Peaks / Ratio / Ret. Tine
Compound/
M_Z.... QC.Log Omit Why ..RT. OK Ratio Total.Area... Area.Peak.1.. Area.Peak.2.. Rel.RT Compound.Name.. ID.. Flags.
DC SN 32:36 RO 0.54 0.28 0.944
DC SN 32:52 0.96 1.37 0.952
DC SN 33:00 RO 0.71 0.74 0.956
DC SN 33:04 RO 0.74 1.23 , 0.958
DC SN 33:10 RO 0.40 1.04 . 0.960
DC SN 33:47 RO 0.38 0.79 '' 0.978
DC SN 34:15 RO 1.49 1.19 0.992
34:39 0.88 19.66 9.19 10.47 1.0030CDF AN
DC SN 34:55 RO 8.43 0.57 1.011
DC SN 35:13 RO 0.23 0.30 - 1.020
DC SN 35:30 RO 1.65 0.49 1.028
442-444 1 Peak 19.66
OCDD 0.76-1.02 0.884-1.116
458-460 DC NL 0:00 RO 1.17 0.11 0.000
34:33 0.86 22.70 10.48 12.22 1.000 OCDD AN
DC SN 34:59 RO 0.48 1.78 1.013
458-460 1 Peak 22.70
13C12-OCDD 0.76-1.02 0.995-1.005
470-472 DC NL 0:00 1.00 0.16 0.000
34:32 0.81 1,430.19 63i.80 791.39 1.000 13CT2-OCDD 189
470-472 1 Peak 1,430.19
Column Description "Why" Code Description QC Lag
M_Z -Nominal Ion Hass(es) WL-Below Retention Ti»e Window A-Peak Added
..RT. -Retention Time (BIB:SB) HH-Above Retention Tiae Window K-Peak Kept
Rat.l -Ratio of M/M+2 Ions SN-Below Signal to Noise Level 0-Peak Deleted
OK -RO-Ratio Outside Limits
-------
F±latS975816 tl-848 Acq:ll-SEP-1997 03:46:13 EI+ Voltage SIX 70S «oif»:227
303.9016 F:2 BSUB(256,30,-3.0) PXJ>(9,5,S,0.05*,908.0,1.00*,r,T) ExptXPCUS
TRIANGLE LASS Text:0-M23-fS TLI143057 ItKT. TIMX - 03:48
OJ
'l7«00 18»00 ia«00 20sOO 21JOO
Til*:S975816 fl-848 Acqtll-SEP-1997 03:46:13 EH- Voltage SIX 70S Ntil*»,335
305.8987 T,2 BSUB(256,30,-3.0) PXD(9,5,5,0.05\,1340.0,1.00\,r,T) Exp:XPCVS
TRIANGLE LABS Text:0-H23-n TLI943057 OKT. TIMX - 03:48
1001
22>00
17:00 IfliOO 19:00 20:00 21:00
rile:S97S816 tl-848 Acq:ll-SEP-1997 03:46:13 EI+ Voltage SIX 70S Noi**,37
315.9419 Ts2 BSUS(256,30,-3.0) PKD(9,5,5,0.05\,148. 0,1. 00\,r,T) ExptEPCUS
TRIANGLE LABS Text:O-M23-rB TLI943057 HKT. TIMX - 03:48
1001 A9.54E6
80:
60:
40:
20:
22:00
17:00 18,00 15.00 20:00 21>00
File:S975816 tl-848 Acqill-SEP-1997 03:46:13 EI+ Voltage SIS 70S Noif»,252
317.9389 Ts2 SSUB(256,30,-3.0) PKD(9,5,5,0.05\,1008.0,1.00\,T,T) Ezp:EPCUS
TRIANGLE LASS Text:O-M23-n TLH43057 OKT. TIME - 03:48
1001
80:
20
22:00
21:00
17:00 18:00
F±le:S975816 tl-848 Acqsll-SEP-1997 03:46:13 EH- Voltage SIS 70S
330.9792 r:2 ExpsEPCVS
TRIANGLE LABS Teit,O-M23-FB TLIf43057 IWJ. TIME -
1001
03s 49
80:
60:
40:
20:
0.
21 : 4222: 01
17,50
if.«0
17:00 18:00 19:00 20:00 21:00
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375.8364 F:2 Exp:EPCUS
TRIANGLE LASS Tejct:O-M23-FB TLH43057 ZK7. TIME - 03,48
23:00
Tim»
3X6
exs
3X6
8X5
4X5
0X0
Tim*(
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4X6
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-------
File -.5975816 41-848 Acqi ll-SEP-1997 03:46:13 EI+ Voltage SIR 70S Hairnet 32
339.8597 Ft2 BSOB(256,30,-3.0) PKD(7,5,3,0.05\,128.0,1.00\,F,T) EiptEPCUS
TRIANGLE LABS Text:0-M23-FB TLIt43057 1X7. TIME - 03:48
1001
aol
40:
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A8.62E4
A2.05E4 AS. 93X4 1
A1.72E4 A2.27E4 \ ifl A3.25E4 ll
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341.8567 F:2 BSUB(256, 30, -3.0) PKD(7,5,3,O.OS\,748.0,1.00\,F,T) EiptEPCUS
TRIANGLE LABS Text:O-M23-FB TLIt43057 1X7. TIMX - 03:48
1001
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sol
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A5.48E4 , „_.
f A5.79E4
ll A6.72E4 1
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File:S975816 tl-848 Acq: ll-SEP-1997 03:46:13 EH- Voltage SIR 70S Noise 1 33
351.9000 Ft2 BSUB(256,30,-3.0) PXD(7,5,3,0.05\,132.0,1.00\,F,T) XxptXPCOS
TRIANGLE LABS Text:O-M23-FB TLH43057 1X7. TIME - 03*48
1001
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60:
40:
20:
0:
A1.08E7 A1.14E7
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Tile:S975S16 tl-848 Acq: ll-SEP-1997 03:46:13 XH- Voltage SIR 70S Noiaet40
353.8970 F:2 BSUB(256,30,-3.0) PJO)(7,5,3,0.05\,160.0,1.00\,F,T) ErptEPCUS
TRIANGLE LABS Teit:0-M23-FB TLIt43057 HKT. TIKE - 03*40
1001
•
so:
sol
401
201
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A7.61ES
A6.56X6 U
ft
/ V / v
-2.4X6
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0.0X0
23:00 34*00 ' 35*00 35*00 Time
File:S975816 tl-848 Acq: ll-SEP-1997 03:46:13 EH- Voltage SIR 70S
330.9792 Fs2 ExpiEPCUS
TRIANGLE LABS TextiO-H23-FB TLH43057 1X7. TIME - 03:48
1001
aol
60".
40:
201
o-
^ ^^iiii-^v-^^^V^^^
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0.0X0
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FilmtS975816 tl-848 Acq: ll-SEP-1997 03:46:13 XH- Voltage SIR 70S
409.7974 Fi2 ExptEPCUS
TRIANGLE LABS TextsO-M23-FB 2X7*43057 1X7. TIME " 03t48
1001
aol
60l
40:
201
ol
34*31
1
34*51
i 3fe,0tf «'« J.5'*' 35.05 26,33**' 39
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33*00 ' 34*00 35*00 35*00 ' ' ' ' Tim*
— - - • •
211
-------
Fne,S97Saie U-HB Acq:lT-s£P-1997 03,46:13 Sl-t- Volttg* SOt 70S Noim*t345
355.8546 F:2 BSUB(256, 30, -3.0) PKD(7,5,3,0.05\,1380.0,1.00\,F,T) Xxp:XPCOS
TXIANGLE LABS Text:O-M23-FB TL1I43057 UW. TIMX - OJ»48
1001 A6.04E4
1 i fii °ttn
80J 1 j A3.81E4 A3.58E4 ..-
J ft 1 i I A4 . 71£4
J ill m H i \ A1.08E4
\ nil 1 II ft 1 II A1.79X4
40\ 111 AIT" w 11 A1'\Ei fill , IU-*»«U ii
aoJI — 11 1 L 11 nr.3Vt3\ 1 — Mi. T~n ITT 1 1 HI A IU h A ill IT AJ..J.J&I TTT
24 ',00 ' 25:00 26\00
.1.6X4
""*
3.5X3
.6.3X3
.2X3
0.0X0
X±m»
FJL1»:S975816 #1-848 Acqill-SEP-1997 03:46:13 EI+ Volt*9» SI* 70S Moimm:27
357.8516 F:2 BSOB(256, 30, -3.0) PXD(7,5, 3,0 .05\, 108.0, 1.00\,T, T) BxpiEPCUS
TXIANGLE LABS Text:0-M23-FB TLIt430S7 IKT. TIMX - 03«48
1003
801
601
401
201
A1.S7X5
A4 . 62E4
A A3. 67X4 A3.UX4
A /V A1.07W A7.84X3
24:00 ' ' . 25:00 26:00
.6.8X4
.5.4X4
.4.1X4
.2. 7X4
.1.4X4
'0.0X0
Timm
Fil»:S975816 #1-848 Acq, ll-SEP-1997 03:46:13 Eli- VoltMym SIX 70S Boim»i44
367.8949 F:2 BSUB(256,30,-3.0) PKD(7, 5, 3, 0.051,176. 0,1.00*^,1) ExptETCDS
TXIANGLE LABS T*JCttO-M23-FB TLIH3057 3JET. ZZtV - 03i4»
1003
801
60.
40.
20.
A7.03X6 .
n
ft
1
I k7.31Z5
y WV
-3.4X8
J..9X6
.1.4X6
.9.4X5
.4.7X5
O..OEO
24[sOO ' 25 1 00 26:00 Timm
F±la:S975816 #1-848 Acqtll-SEP-1997 03:46:13 XI+ Voltage SIX 70S Soif»:3S
369.8919 F:2 BSUB(256,30,-3.0) PX>( 7,5, 3,0 .05\,140.0,1.00\,F,T) ExptEPCUS
TXIANGLE LABS Text:0-H23-FB TLH43057 IJKT. TIME - 03s48
10 Oi
80.
60.
40_
20.
0
A4.B7E6
n
ft
1
/ A4 . 63E5
1 \yv
24:00 25:00 26:00
1.6X6
'.1 . 3X6
.9.7X5
.6.5X5
.3.2X5
0.0X0
Tim
File:S975816 #1-848 Acqill-SEP-1997 03:46:13 EI+ Volttge SIX 70S
330.9792 F:2 ExptEPCOS
TS I ANGLE LABS TfXt:0-M23-FB TLIf 43057 IXT. TIME - 03:48
1003
80.
60.
40.
20.
24:00 34,JJ^^^^4^24,59 25j£8^^JSjJJ^^™,01 v^3&&~J6,42^
s_A^^-\^-'v^*>^' ^->xvv Y \r
-.1.2X7
.9.8X6
.7.3X6
.4.9X6
.2.4X6
0.0X0
24\00 ' ' 25>00 ' ' 26\00 Tl*
212
-------
File,S975816 tl-406 Acqill-SEP-1997 03,46,13 ZI+ VoltMgm SIS 70S Noiam,651
373.8208 T,3 BSUB(256,30, -3.0) PXD( 7, 5, 3, 0.05\,2604.0,1.00\,r,T) Xzp:XPCUS
TRIANGLE LABS Tmxt:O-M23-TB TLH430S7 IOJ. TIHX - 03l48
1001
80:
en •
D l/_
40J
20-
Al.
A1.22X5
n
A5.60E4I 1
/ r9 ' ?3Z3 H A2.48E4 f
I \ A ^vJL.A'V rJ
12X5
1 A9.22E4
l\ *, 11*4 I
f\J^E* J\A / \ A1.92E4 /V /M A8.55E3
27\12 27:24 27', 36 27': 4 8 28:66 28', 12 28:24 28:36 28:48 29:00 29\12 29\'24 2 9', 3 6 29:48 30',66 30ili
_5.4M
_4.JJE4
. J • 2JC4
2.2.E4
.I.XE4
; H»«
rilm,S975816 tl-406 Acqtll-SXP-1997 03:46,13 EH- VoltMgm SIS 70S Hoimm,349
375.8178 T:3 BSUB(256,30,-3.0) PXD(7,5,3,0.05\,1396.0,1.00\,F,T) ExptSPCOS
TRIANGLE LABS Text:O-H23-FB TLIt43057 XK7. TIHX - 03,48
1003
ao:
60:
'
4°-.
20-
Al.
AS. 33X4 I
ft
A3 . 79X4 \ 1
11 f
14X5
1
n A7.59X4
1 ft
111 11 a 3 o-rvf
A /I ~'i"jb 8SE4 / II \ A2.93E4 J 1, 1,
r\ i/ \A9.20X3k AJ;j?ar1 / U \ M . >> J |T.ffffM A4.11X3lT\!L ,, ««
^^—7 AA 1* ViATJX/W* SAv-^^WVvJU ^ fJ\J ^ \fS ' VVU^/ 1 W /" ' VV, Jb /^j^s^ -*s ^ta*^\-* -^ ^ ' ^^-^A rt rtf ^fi
27:12 271: 24 27:36 -27.48 28166 2aYl2 28:24 28.-jtf 28:48 29', 66 29,12 29 ,24 29', 36 29', 4 8 jb.'oO 30:11
«.0n
13.2X4
12.4-X4
*
-.1.6E4
.7.9X3
1 Time
rilm:S975816 tl-406 Acqtll-SXP-1997 03:46:13 EH- VoltMgm SIS 70S Ooimm:472
383.8639 7:3 BSVS(256,30,-3.0) PXD(7,5,3,0.05*,1888.0,1.00\,r,T) ExptEPCUS
TRIANGLE LABS TmxtiO-M23-fB TLH43057 UKT. TIHE - 03:48
1003
ao:
eo:
40:
20:
0'
27
A5.f7E6 A4.f8X6
1
A A
/ «.8JIff
A
vl /I /V
,12 27,24 27',36 27,48 28:66 28:12 28',24 28: 36 ' 28:48' 29\ Oo' 29:12' 29:24 ' 29\ 36' 29',48' 's'oVoo' 30:L
-1.8X6
Li.aw
Ll.IZff
-.7.3X5
.3.6X5
-.0.0X0
I Timm
rilm:S975816 tl-406 Acq:ll-SEP-1997 03:46:13 EH- Volt»ge SIS 70S Hoi3° 30'06
37,16 \ 38:05 1 "l44 29:5B
1 111 \7l51 ! 1 1 *"«' llfll »SU 1 ,1 , ill . 1
U/ybuyiLiiJi^^
U'U 'IKJU' VvlUww H'VWUIftVul U ULJUN>^l/wV<4_A/sJVir'iHwSU>UU Vlll U"JW "<-l'<*&f*J WUI W^J l^^v*' N/UwiA/l w W.
27:12 27:24 27:36 27:48 28:00 28',12 28\24 28^36' 28\48' 29:66 29:12' 29\ 24' 29\ 36 29: 4t 30:00 30',i
-4.8X3
-.3.8X3
•2 9X3
.1.9X3
.9.6X2
-.0.0X0
1 Time
213
-------
ro
-------
File,S975816 #1-430 Acq:ll-SEP-1997 03:46:13 EH- Voltage SIX 70S Noi»e,413
407.7818 F,4 BSUB(256r30, -3.0) PKD(7,5,3,0.05\,1652.0,1.00\,r,T) ExptXPCUS
TRIANGLE LABS Text:O-M23-FB 2X1*43057 1ST. HUE - 03t48
1004 A2.38E5
80:
60:
40:
20:
A6.62S4
31:24 31:36 31:48 32,00 32,12 32,24 32,36
Flle:S975816 H-430 Acq:ll-SEP-1997 03,46,13 XI+ Voltage SIS 70S Boil*1164
409.7789 F,4 SSUB(256,30, -3.0) PXD(7,5,3,0.05\,656.0,1.00\,r,T) XacpiXTCUS
TRIANGLE LABS TejCt:0-M23-FB TLIf43057 1ST. TIME - OJl4fl
1004 A1.76E5
80:
60l
3248
40:
20:
o.
A4.74E
A5.49E4
E4 A
j W
A6.52E4
9.7X4
7.7X4
5.8E4
.3. 9E4
.1. 9X4
.0.0X0
Tia,
.5.5X4
.4.4X4
.3.3X4
.2.2X4
.1.1E4
.0.0X0
31,12 31,24 31,36 31,48 32,00 32,12 32,24 32,36
File,3975816 tl-430 Acq:ll-SEP-1997 03,46,13 EI+ Voltage SIS 70S Soiae,477
417.8253 F:4 BSUB(256,30,-3.0) PKD(7 ,5,3 ,0.05\,1908.0,1.00\,F,T) KxpiXPCUS
TRIANGLE LABS T*xt:O-M23-FB TLH43057 XK7. TIKE - 03,48
1004 A3.23E6
80:
601
40:
20:
32:48
31,12 31,24 31,36 31,48 32,00 32,12 32,24 32,36
Flla:S975816 tl-430 Acqtll-SEP-1997 03,46,13 EI+ Voltage SIS 70S XOiff>333
419.8220 F,4 BSUB(256,30,-3.0) PRD(7,5,3,0.05\, 1332.0,1.00\,F,T) XrpiXPCUS
TRIANGLE LASS Text,0-M23-FB TLIt43057 JK7. TIME • OJi48
1004 A7.60E6
32: 48
80.
60:
40:
20:
AS.00X6
31,12 31,24 31,36 31,48 32,00 32,12 32,24
F±le,S975816 tl-430 Acq,ll-SEP-1997 03,46,13 EH- Voltage SIS 70S
430.S729 F,4 ExptEPCUS
TRIANGLE LABS TeJCt,O-M23-FB TLIf43057 IXT. TIKE - 03,48
1003
60:
40:
20:
o:
33,a5
32:36
32,38
32:48
31:12 31,24 31:36 31,48 32:00 32,12 32:24
Til»tS975816 tl-430 Acqtll-SXP-1997 03,46:13 EI+ Voltage SIS 70S
479.7165 F:4 XxpiXPCUS
TRIANGLE LABS T»xt:O-H23-FB TLH430S7 IXT. TIME - 03:48
1001 31f57
80:
60:
40:
20:
0:
32:36
32:48
32,41. 33'49
1.1E6
8.9X5
.6.7X5
.4.5X5
.2.2X5
.0.0X0
Time
.2.6X6
.2.1X6
.1. 6X6
.1.1X6
.5.3X5
.0.0X0
31,12
31,24
31:36
31,48
32,00
32:12
32124
32,36
32,48
4.6X6
3. 6X6
2.7E6
.1. 8X6
9.1X5
0.0X0
Tin*
.1.8X4
.1.4X4
.1.1X4
.7.0X3
.3.5X3
0.0X0
Tin el
215
-------
'ile:S975816rl-430 AcqtlJ.-SEP-J.SS7 03:46:13 El+ Voltage SIS 70S Holmfi173
423.7766 rt4 BSUB(256,30, -3.0) PXD(7,S,3,0.05\,692.0,1.00\,r,T) fxp.EPCVS
TRIANGLE LASS Taxt,O-M23-TB TLI»43057 IJW. TIME - 03:48
1004
80.
60.
40.
20.
31:18 31i24 31s30 31:35 31i42 31i48 3ls54 33iOO 32:06 32:12 32:18 32t24 32130
riletS975816 41-430 Acqtll-SEP-1997 03:46(13 fl+ Voltagm MIX 70S Xoi**t213
425.7737 f:4 BSOS(256,30,-3.0) PKD(7,5,3,0. OS*, 852.0,1.00\,r,T) XxptEPCUS
TRIANGLE LABS T*xt:O-M33-FB TLH43057 2X7. TIME - 03t48
100* A1.01X5 -3.4X4
A8.29E4
A1.19ES
A6.10E3
A4.25X3
A8.56S3
A
A3.43X4
,3.1E4
-2.5E4
-1.9E4
.1.3E4
-6.2E3
O.OEO
00:
so:
40'.
20:
A6.45E4
A6.21X3
A
A7.13E3
AS.36E3
^ A
.2. 7E4
.2.0X4
.1.4X4
.6.8E3
31,18 31t24 31,30 31:36 31:42 31:48 31:54 33*90 32,06
f±leiS975816 tl-430 Ac40 31:54 32:00 32,06 32:12 32:18
rile:S975816 #1-430 Acqtll-SEP-1997 03:46*13 XI+ Voltage SIX 70S Boiu*:811
437.8140 T:4 BSUB(256,30,-3.0) PKS(7,5,3,0.05^,3244.0,1.00\,T,I) ErptEPCOS
TRIANGLE LABS Text:O-M23-n TLH430S7 UKT. TIME - 03:48
1001 A5.99E6
801
60.
40.
20.
32,24 32:30
.2. 9X6
11.5X6
'.1.1X6
17.5X5
.3 . 7X5
31:20
31*10 31,24 31:30 31:36 31:42 31:48 31:54 32:00 32,06 32:12 32:18 32,24 32:30
rile,3975816 41-430 Aoq:ll-SEP-1997 03,46>13 EH- Voltage SIS 70S
430.9729 r,4 ExptEPCVS
TRIANGLE LASS T*xt:O-M23-TB TLIt43057 UKT. TIMX " 03,48
1001
80.
60.
40.
20.
0.
O.OEO
Time
.4.3X6
.3.5X6
.2.6X6
.1.7X6
.8.7S5
0.0X0
31:18 31:24 31:30 31:36 31:42 31:48 31,54 32:00 32:06 32:12 33:18 32:24 32,30
Tim*
216
-------
File:S975816 tl-430 Acqtll-SEP-1997 03:46:13 EI+ Voltage SIS 70S Noise:32
441.7438 Ft4 BSUB(356,30,-3.0) PKD(7,5,3, 0.05\, 138.0,1.00\,F,T) XrptXPCOS
TRIANGLE LABS TeittO-H23-FB TLH43057 JMT. TIME -
1001
03148
31100 32100 33:00 34tOO
FilesS975816 tl-430 Acqtll-SEP-1997 03:46il3 EH- Voltage SIR 70S Jfoi»e:30
443.7399 T:4 BSUB(356, 30,-3.0) PXD(7,5,3, 0.05\,120.0,1. Q0\,r, T) ExptEPCUS
TRIANGLE LABS Teit:0-M23-FB TLH430S7 I2KT. TIMS - 03:48
Al.OSES
35100
3ltOO 32:00 33:00 34': 00
rile>S975816 tl-430 Acqtll-SEP-1997 03:46:13 EI+ Voltage SIS 70S
430.9729 Ts4 ExptEPCUS
TRIANGLE LABS Text:O-H33-PB TLH43057 UKT. TIME - 03:48
33{00 33t37 ii.nn 34:33
35:00
1003
901
801
701
601
501
401
301
2o'l
101
01
34:00
15*17
30:46 31t07
31:49
Time
-4.6X6-.
.4.1X6
''.3. 7X6
.3.2X6
.2.7X6
.2.3X6
.1.8X6
'.1.4X6
.S.1XS
.4. 6X5
0.0X0
31:00 32:00 33:00 34:00
Flle:S975816 f 1-430 Aojtll-SEP-1997 03:46:13 EI+ Voltage SIX 70S
513.6775 F:4 ExptEPCPS
TXIANGLE LABS Text:O-H23-FB TLH43057 JJK7. TIME "
1001
901
801
701
601
501
35100
03:48
301
201
101
" "
31,05 3it38
JsMJ^jk^
33,51
UJ
34136
34159
34125
35:3'
35123
31\00
33:00
33'tOo'
34', 00'
35100
-S.3X3
.8.4X3
-.7.5X3
16.5X3
.5.6X3
'.4.7X3
.3.7X3
.3.8X3
.1.9X3
.9.3X2
0.0X0
Time
217
-------
lie:SST5B16 ti-430 AcyiIJ.-SEf-J.997 OJ:46sJ.J Eli- Voltage SIX 70S Noi»et34
457.7377 F>4 BSUB(256,30, -3.0) PKD(7,5,3,0.05\r136.0,1.00\,r,T) XxpiXPCOS
TRIANGLE LABS Text:0-M23-n TLH430S7 HKT. TIME - 03i48
1001 A1.Q5E5
so:
60J
20.
34124 34s30 34i36 34i42 34:48 34:54
r±letS97SB16 H-430 Acqtll-SEP-1997 03:46,13 EH- Voltmgm SXM 70S mtl*e:28
459.7348 F:4 BSOB(256,30,-3.0) PXD(7,5,3, 0. 05\, 112.0,1.00\,r,T) SxptfPCDS
TRIANGLE LABS TextsO-M23-n TLH43057 JJtT. TIME - 93:48
A8.3SE3
.1. 7E4
-1.2X4
.8.313
'.4.2X3
35:00
0.0X0
Timt
1004
80.
60.
40.
20.
A1.22E5
Al. 75E4
~r
T
I*
.2.SE4
-2.1X4
'.1.5X4
.1. 0X4
'.5.2X3
34:24 34:30 34t36 34:42 34:48 34:54
TJLletS975816 tl-430 Acgsll-SXP-1997 03:46:13 EI+ Voltagm AZX 705 Boim»t39
469.7779 F:4 BSUB(256,30f-3.0) PXD(7,S,3rO.OS\tiU.tri,9t\f*,I) XxptSTCDS
TXIASGLX LABS T*xt:O-M23-fB TLH43057 XXT. 33MV - *3i48
1001 A6.J9E6
ao:
so:
40:
20:
35:00
LO.OXO
Tlmt
34,24 34:30 34:36 34:42 34:48 34:54
F±le:S975816 tl-430 Acqtll-SEP-1997 03:46:13 EH- Voltage SIX 70S Moim»s38
471.7750 T:4 BSUB(256,30,-3.0) PKD(7,5,3, 0.05\,152.0,1. 00\,f,T) EzptEPCOS
TRIANGLE LABS T*xtiO-H23-n TLIt43057 XKT. TIME - 03:48
100\ A7.91ES
801
-I.4Z5
J..3JS6
.8.4X5
.5.6X5
.2.8X5
.0.0X0
35:00 Time
-1. 7X6
'.1.4X6
'.1. 0X6
.6.9X5
.3. 4X5
34:24 34': 30 34:36 34:42 34:48
rile:S975816 tl-430 Acqtll-SEP-1997 03:46:13 EH- Voltage SIX 70S
430.9729 fs4 ElptEPCVS
TSIAHSLE LABS Text.:O-M23-TB TLIt43057 ItKT. TIMS
100& 34:33
ao:
60.
40.
20.
0.
34:54
03:48
35:00
0.0X0
Time
-4.5X6
.3.6X6
.2.7X6
11. 6X6
.9.0X5
34124
34,30
34:36
34142
34148
34154
35:00
.0.0X0
Tim
-------
Chamet I 338,3732 Peak top
Height 3,3 volts Span 288 ppi
Systei file raae EPCUS2
Data fiLenatt fi=$911971
Resolution 18888
Groupnuibef 2
Icnlzatlon lode El"
Switching VOLIBGE
Ref, tasses 292,3825, 416,3768
J 331 S 368
X 332 T 378
I 334 U 376
H 348 V 418
H 342
0 3S2
P 354
Q 356
R 358
Ref, ass 416,9768 Peak top
Height ,72 volts Span 288 ppi
-------
o
CM
CM
File;5975816 1U-B49 Acq;ll-5BP-1997 03:46:13 EI4- Voltage SIR 705
339.8597 F:2 Exp:EPCUS
Sample Text:0-M23-FB TLI143057 INJ. TIME - 03:48 File Text:0-M23-
100%.
FB TLI»
..1.8E4
24 OO' ' 24:12 ' '24:24' ' '24:36 ' 24!48' ' VSiOO 25il2 25i24 25.;36 25:48 26iOO
File:S975816 #1-848 Acq:ll-SEP-1997 03:46:13 EI+ Voltage SIR 70S
341.8567 F:2 Exp:EPCUS
Sample Text:O-M23-FB TLI#43057 INJ. TIME - 03:48 File Text:O-M23
100S.
A3.49E4
O.OEO
Time
FB TLI»
_1.4E4
24 00 24il2 24J24 24i36 24!4B' 25100 25ll2 25:24 25i36 25:48 26:00
File:S975816 #1-848 Acq:ll-SEP-1997 03:46:13 EI+ Voltage SIR 70S
351.9000 F:2 Exp:EPCUS
Sample Text:O-M23-FB TLI#43057 INJ. TIME = 03:48 File Text:O-M23
100S. 24:42 25j.27
60
40J
20J
Oj
24
1 i i i i i 'I i i i 'i i I i i
00 24:12 24:24
24:36
24:77
O.OEO
Time
FB TLI>
3.6E6
_2.9E6
_2.1E6
_1.4E6
L7.2E5
25:00 25:12 25:24 25:36
25:48
26:00
O.OEO
Time
-------
221
-------
CJI
CJ
File:S975816
407.7818 F:4
Sample Text:
100%,
80J
60 j
40J
20J
0:
A
30:48
File:S975816
409.7789 F:4
Sample Text:
1004
80J
60 j
40J
20 j
oj
|FT=visf:>r
30:48
File:S975816
417.8253 F:4
Sample Text:
1004
80J
60J
40J
20J
0:
30:48
#1-430 Acq:ll-SEP~1997 03:46:13' EI4- Voltage Sift 70S
Exp: EPCUS
O-M23-FB TLI#43057 INJ. TIME - 03:48 File Text:0-M23-FB
A2.31E5 r9
1
P
31:00 31:
1
I
12
31:24 31:36 31J48 32:00 32:12 32:24 32:36 32:48 33:00
_7
.5
_3
_0
#1-430 Acq:ll-SEP-1997 03:46:13 EH- Voltage SIR 70S
Exp : EPCUS
0-M23-FB TLI#43057 INJ. TIME = 03:48 File Text:0-M23-FB
A1.75E5 r5
A
31:00 31
V
12
_/\j\_ _____JV_ _^__
L4
:3
.2
0
31:24 31:36 31:48 32:00 32:12 32:24 32:36 32:48 33:00
#1-430 Acq:ll-SEP-1997 03:46:13 EI+ Voltage SIR 70S
Exp : EPCUS
O-M23-FB TLI#43057 INJ. TIME = 03:48 File Text :O-M23-FB
31:10 rl
A
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31:66 31:
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12
32:22
A'
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. 6E4
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Time
-------
File:S975816 #1-430 Acq:ll-SEP-1997 03
423.7766 F:4 Exp:EPCUS
Sample Text:0-M23-FB TLI#43057
lOOi Al.aiE5
;46:13 EI+ Voltage SIR 70S
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03:48 File Text:O-M23-FB TLI>
^3.1E4
31:36 31:48 32:00 32:12
File:S975816 #1-430 Acq:ll-SEP-1997 03
425.7737 F:4 Exp:EPCUS
Sample Text:O-M23-FB TLI#43057
lOOi A9.93E4
80J
60 j
40J
20 j
32:24 32:36 32:48
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33:00
33:12
33:24
Time
31:36 31:48 32:00 32:12
File:S975816 #1-430 Acq:ll-SEP-1997 03
435.8169 F:4 Exp:EPCUS
Sample Text:0-M23-FB TLI#43057
100^ 32L02
80J
60J
40J
20j
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32:24 32:36 32i48
:46:13 EI+ Voltage SIR 70S
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03:48 File Text:O-M23-FB TLI»
3.4E4
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33:00
33:12
33:24
31: 36
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03:48 File Text:O-M23-FB TLI>
1.7E6
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33:00
33:12
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33:24
fO
C*
Cl
-------
TLI Project 43057
Client Sample: O-M23-RB
Method 23 PCDD/PCDF Analysis (a)
Analysis File: S975817
Client Project
Sample Matrix:
TLI ID:
Sample Size:
Dry Weight:
GC Column:
'• ^*T>H/k.T TLAfirr "A"
M23TRAIN
181-27-7AB&*
1.000
n/a
DB-5
Date Received:
Date Extracted:
Date Analyzed:
Dilution Factor:
Blank File:
Analyst
08/29/97
09/06/97
09/11/97
n/a
S975807
HLM
Spike File:
ICal:
ConCal:
% Moisture:
% Lipid:
% Solids:
SPX23704
SF56117
S975814
n/a
n/a
n/a
£rt£titri&^% s *• J*If '^'Hi^'^^**S»5?
25:51
29:11
32:02
3422
2527
28^0
28:28
28:58
29:41
31:11
32:22
34:40
f &t%&wjfyk&i&iifi
fll^iiS^
^^_^^
•^••^
^^ ^^
PR_
B_
B—
B_
^MBB^V
B
PRB
B_ .
PRB
^^i«^B
B_
B_
B_
fjfo$»#&
•H^HIW
Page 1 of 2
X237_PS« »100, LMU &1OM
Triangle Laboratories, Inc.*
801 Capitola Drive • Durham, North Carolina 27713
Phone: (919) 544-5729 • Fax: (919) 544-5491
Printed: 08:1 8 09/1 2/97
224
-------
U Project: 43057
:iient Sample: O-M23-RB
Method 23 PCDD/PCDF Analysis (a)
Analysis File: S975817
Internal Standardisin
C12-2,3,7.8-TCDF
Cl2-2,3,7,8-TCDD
C12-l,2,3,7,8-PeCDF
>C12-lA3,7,8-PeCDD
•C,rl,2,3,6,7,8-HxCDF
C,rU,3,6,7,8-HxCDD
>Cl2-l,2,3.4,6,7,8-HpCDF
>C,2-l,2,3,4,6,7,8-HpCDD
Ci2-U,3,4,6,7,8,9-OCDD
3.5
3.1
3.6
4.0
3.0
3.1
2.5
4.9
88.5
76.4
89.1
99.3
74.0
78.2
56.7
61.3
60.9
40%-130%
40%-130%
40%-130%
40%-130%
40%-130%
40%-130%
25%-130%
25%-130%
25%-130%
0.75
0.82
1.46
1.55
0.46
1.22
0.43
1.01
0.79
20:21
21:10
24:41
25:49
28:27
29:11
31:10
32:01
34:32
Surrogate Standards {Type Af
'Or2,3,7,8-TCDD
>Ca-2,3,4,7,8-PeCDF
JC12-lA3,4,7,8-HxCDF
!C,2-lA3,4,7,8-HxCDD
!C12-lA3,4,7,8,9-HpCDF
5C,rlA3,7,8,9-HxCDF
43
4.1
3.6
3.7
3.6
2.7
3.1
107
102
90.2
91.6
89.0
70%-140%
70%-140%
70%-140%
709b-140%
70%-140%
1.49
0.48
1.22
0.44
21:12
25:27
28:20
29:05
32:22
66.8
76.9
40%-130%
40%-130%
0.46
0.48
29:40
28:58
%, ,<,
Recovery StancfanlS;
3C,2-1A3,4-TCDD
0.88
1.20
20:58
29:28
Duality Control Notes:
' 181-83-1
Date Received (181-83-1): 09/05/97
Data Reviewer.
Page 2 of 2
09/12/97
X237_RK •240.LAIB4UUM
Triangle Laboratories, Inc.*
801 Capitola Drive • Durham, North Carolina 27713
Phone: (919) 544-5729 • Fax: (919) 544-5491
Printed: 08:18 09/12/97
Jk . 225
-------
Data Review By:
•Calculated Noise Area:
1.44
The Total Area for each peak with an ion abundance ratio outside
ratio limits has been recalculated according to method requirements.
Page No.
09/12/97
Listing of S975817B.dbf
Matched GC Peaks / Ratio /
Ret. tiae
Compound/
M_Z QC.Log Omit Why ..RT. OK Ratio Total.Area... *r«a. Peak. 1.. Area.Peak.2.. Rel.RT Compound.
ID.. Flag*.
TCDF
304-306
D
M
304-306
13C12-TCDF
316-318
316-318
TCDD
320-322
D
DC
DC
DC
DC
DC
D
DC
DC
DC
DC
DC
DC
DC
DC
D
DC
DC
DC
DC
DC
DC
DC
DC
DC
DC
DC
DC
DC
DC
NL
SN
SN
SN
SN
SN
SN
SN
SN
SN
1
NL
WL
4
NL
SN
SN
SN
SN
SN
SN
SN
SN
SN
SN
SN
SN
SN
SN
SN
SN
0:00
16:51
18:00
18:26
19:13
19:31
20:23
20:36
20:52
21:07
22:18
Peak
0:00
19:10
19:30
19:53
20 : 21
20:51
Peaks
0:00
18 : 16
18:24
18:43
18:59
19:03
19:10
19:16
19:26
19:36
19:52
20:06
20:37
20:42
20:54
21:05
21:13
21:24
0.
RO
RO
RO
RO
RO
65-0.89 ' .
0.11
4.
0.
,04
.18
1.27
0.57
0.80
RO
RO
RO
RO
RO
0.
.61
0.13
0.18
0.36
1.58
0.
18
0.48
0.94
3.29
3.13
5.63
8.94 3.89
0.25
0.85
2.87
2.34
0.820-1.101
0.
0.
0.
0.
0.
0.
6.42 1.
1.
1.
000
828
885
906
944
959
002
012
025
2378 -TCDF
1.038
1.096
8.94
0.
RO
65-0.89
0.13
0.88
0.65
0.
RO
RO
RO
RO
RO
RO
RO
RO
RO
RO
RO
RO
RO
RO
0
0
0
.81
.75 4,
.78
4,
65-0.89
1
1
0
0
1
1
0
2
0
0
0
2
4
1
0
1
0
2
.50
.02
.66
.83
.80
.55
.24
.40
.78
.27
.87
.69
.22
.32
.44
.38
.42
.04
0.21
25.07
6.98 2.94
20.74 ».29
446.87 1.900.95
26.08 11.39
0.951-1.049
0.000
0.942
4.24 0.958
XI. 45 0.977
2,5*5.92 1.
.000
13C12-2378
14.69 1.025
500.67
0.11
10
0
7
0
0
0
0
0
0
4
0
0
1
1
2
3
0
.51 6.08
.83
.86
.71
.90
.44
.44
.48
.48
.08
.74
.41
.36
.13
.41
.49
.80
0.853-1.059
0.000
5.94 0
.863
0.869
0
0
0
.884
.897
.900
0.906
0.910
0
0
0
0
0
0
0
0
1
1
.918
.926
.939
.950
.974
.978
.987
.996
.002
.011
2378-TCDD
AN
Triangle Laboratories, Inc.® Analytical Services Division
801 Capitola Drive • Durham. North Carolina 27713
Phone: (919) 544-5729 • Fax: (919) 544-5491
Printed: 08:19 09/12/97
226
-------
Page No.
09/12/97
Listing of S975817B.dbf
Hatched GC Peaks / Ratio / Ret. Time
Compound/
M_Z.... QC.Log Omit Why ..RT. OK Ratio Total.Area... Area.Peak.1.. Area.Peak.2.. Rel.RT Compound.Name.. ID.. Flags.
320-322
37C1-TCDD
328
328
13C12-TCDD
332-334
332-334
PeCDF
340-342
D
A
D
H
D
D
340-342
DC
DC
DC
DC
SN
SN
SN
WH
1
21:30
RO
21:56
22:22
22:34
RO
RO
1.
.00
0.84
0.33
1.11
Peak
0.50
1.23
0.57
0.94
10.51
1.016
1.036
1
1
.057
.066
0.906-1.094
DC
DC
DC
DC
DC
DC
DC
DC
DC
D
D
DC
DC
D
DC
DC
DC
D
DC
NL
SN
SN
3
NL
4
NL
SN
SN
SN
SN
SN
SN
SN
SN
SN
SN
SN
SN
SN
WH
4
0
19
21
21
21
22
:00
:38
:12
:31
:38
:01
Peaks
0
19
20
21
21
:00
:52
:58
:10
:32
0.
RO
RO
2,
2,
0.06
9.52 9.52
813.25 2,813.25
2.95 2.95
1.79
1.15
825.72
65-0.89
25
0
0
0
1
Peaks
0
22
22
23
23
23
23
23
24
24
24
25
25
25
25
25
26
26
26
:00
:35
:48
:00
:16
:39
:48
:57
:09
:42
:54
:00
:27
:38
:48
:55
:06
:28
:54
1.
RO
RO
RO
RO
RO
RO
RO
RO
RO
RO
RO
RO
RO
RO
RO
RO
.00
.75
.88 3,
.82 3,
.25
6,
32-1.78
0
1
0
0
0
0
1
1
3
1
0
1
1
1
0
0
0
0
1
.14
.96
.31
.60
.43
.81
.81
.16
.34
.23
.75
.32
.54
.05
.58
.58
.89
.95
.38
Peaks
0.12
18.99 8.11
814.33 1,789.34
105.96 1,398.93
49.12 34.58
988.40
TCDD / PeCDF Follovs -•
0.13
5.10
0.36
1.96
0.94
5.05
17.44 12.40
4.80
1.20
8.46 5.14
2.80
11.43
21.27 12.91
9.84 5.98
0.79
2.68
1.12
5.68
1.38
57.01
0
0
1
1
1
1
.000
.928
.002 37C1-TCDD
.017
.022
.040
SDR1
0.906-1.094
0
10.88 0
2,024.99 0
1,707.03 1
27.75 1
0.907
0
0
0
0
0
0
6.84 0
0
0
4.17 1
1
1
8.36 1
5.70 1
1
1
1
1
1
.000
.939
.991 13C12-1234-TCDD
.000 13C12- 2378 -TCDD
.017
-1.078
.000
.915
.924
.932
.943
.958
.964
.970
.978
.001 12378 -PeCDF
.009
.013
.031 23478-PeCDF
.038
.045 •
.050
.057
.072
.090
RSI
IS1
AN
AN
13C12-PeCDF 1.32-1.78
352-354 DC NL 0:00 RO 1.13 0.15
23:47 RO 1.29 39.27 23.87
24:20 1.75 20.78 13.23
24:41 1.46 3,850.99 2,284.48
0.838-1.162
0.000
18.48 0.964
7.55 0.986
1,566.51 1.000 13C12-PeCDF 123 IS2
Triangle Laboratories, Inc.® Analytical Services Division
(01 Capitola Drive • Durham, North Carolina 27713
'hone: (919) 544-5729 • Fax: (919) 544-5491
Printed: 08:19 09/12/97
u. 227
-------
Page No.
09/12/97
Listing of S975817B.dbf
Hatched GC Peaks / Ratio /
Ret. Ti»e
Compound/
M_Z.... QC.Log Omit Why ..FT. OK Ratio Total.Area... Area.Peak.1.. Area.Peak.2.. Rel.RT Compound.Name.. ID.. Flags.
352-354
PeCDD
356-358
356-358
13C12- PeCDD
368-370
368-370
HxCOF
374-376
D
D
D
DC
DC
DC
DC
DC
DC
DC
DC
DC
DC
DC
DC
DC
DC
DC
DC
DC
D
DC
D
D
DC
DC
DC
SN
SN
7
NL
SN
SN
SN
SN
SN
SN
SN
SN
WH
4
NL
SN
SN
2
NL
SN
SN
SN
SN
SN
SN
SN
SN
24
25
25
25
26
26
:59
:27
:49
:55
:06
:27
RO
RO
RO
RO
1.
1.
0.
1.
1.
0.
Peaks
0
23
24
24
24
24
25
25
25
25
25
25
26
26
:00
:57
:08
:17
:42
:52
:04
:13
:22
:31
:39
:51
:05
:47
1.
RO
RO
RO
RO
RO
RO
RO
RO
RO
RO
32-
14.
1.
9.
3.
1.
1.
2.
8.
1.
2.
1.
1.
0.
4.
38
49
82
89
09
89
1.78
29
41
81
21
47
21
22
85
35
80
12
70
51
84
Peaks
0
24
25
25
26
:00
:41
:49
:58
:08
1.
RO
RO
34.
3,791.
5.
4.
3.
10.
61 20.09 14.52
96 2,267.29 1,524.67
73 3.48
69
64
53 6.40
4.25
7.23
1.012
1.031 13C12-PCCDF 234 SUR2
1.046
1.050
1.057
1.072
7,753.87
0.
13.
0.
0.
15.
2.
9.
0.
2.
2.
2.
7.
1.
0.
45.
18
85 1.11
41
61
46 9.21
78
44 8.23
«
37
98
39
21 4.54
35
79
96
32-1.78
1.
0.
1.
1.
2.
Peaks
0
27
27
27
27
27
28
28
28
28
28
29
29
29
:00
:21
:30
:38
:49
:59
:20
:28
:34
:47
:58
:06
:10
:17
1.
RO
RO
RO
RO
RO
RO
43
78
55
60
39
05-1.43
2.
1.
1.
0.
1.
0.
1.
1.
1.
1.
1.
3.
2.
0.
82
10
21
93
15
40
25
19
26
32
20
03
41
40
0.
2.
2,405.
228.
4.
17
24
29 1,463.62
84 140.66
82
0.921-1.026
5.74
6.25
3.70
2.C7
0.
941.67
18.18
0.000
0.928
0.935
0.941
0.957
0.963
0.971
0.977
0.983
0.988
0.994
1.001 12378-PeCDD Ul
1.010
1.037
845-1.155
0.000
0.956
1.000 13C12- PeCDD 123 I S3
1.006
1.012
2,634.13
1.
19.
40.
2.
8.
1.
60.
30.
8.
10.
28.
0.
0.
0.
34
SO 10.20
31 22.07
69
35
90
57 33.66
75 16.69
31
54
41 15.50
69
87
45
0.
9.30
18.24
26.91
14.06
955-1.052
0.000
0.961
0.967
0.971
0.978
0.984
0.996 123478-HzCDF AN PR
1.001 123678-HxCDF AN
1.004
1.012
12.91 1.018 234678-HxCDF AN PR
1.023
1.025
1.029
Triangle Laboratories, Inc.® Analytical Services Division
801 Capitola Drive • Durham, North Carolina 27713
Phone: (919) 544-5729 • Fax: (919) 544-5491
Printed: 08:19 09/12/97
-------
ige No. 4
9/12/97
Dmpound/
_Z. . . . QC. Log Omit Why
Listing of S975817B.dbf
Matched GC Peaks / Ratio / Ret. Time
.RT. OK Ratio Total.Area... Area.Peak.1.. Area.Peak.2.. Rel.RT Compound.Name.. ID.. Flag*.
74-376
3C12-HXCDF
84-386
84-386
xCDD
90-392
D
M
90-392
.3C12-HXCDD
02-404
.02-404
DC SN 29 : 28
29:41
29:46
DC SN 29:53
DC WH 30:01
DC WH 30:12
7 Peaks
DC NL 0:00
DC SN 27 : 20
27:28
28:20
28:27
DC SN 28:41
DC SN 28:44
28:58
29:40
DC SN 29 : 57
5 Peaks
DC NL 0
DC SN 27
27
DC SN 28
DC SN 28
28
28
DC SN 28
D SN 29
29
DC SN 29
29
DC SN 29
DC WH 29
DC WH 29
DC WH 29
:00
:46
:53
:04
:09
:35
:57
:06
:18
-.28
:35
:40
:50
:52
RO 0.82 0.76 1.036
1.33 6.37 3.64 2.73 1.043 123789-HxCDF AN
RO 1.49 13.08 8.70 5.84 1.046
RO 2.29 1.01 1.050
RO 0.80 0.72 1.055
RO 1.62 0.65 1.062
198.99
0.43-0.59 0.859-1.141
RO 1.22 1.86 0.000
RO 0.40 6.01 0.961
RO 0.66 15.89 6.94 10.52 0.965
0.48 2,718.04 884.25 1,833.79 0.996 13C12-HXCDF 478 SDH3
0.46 3,143.19 997.30 2,145.89 1.000 13C12-HXCDF 678 IS4
RO 0.71 4.79 1.008
RO 0.26 4.47 1.010
0.48 3,022.43 985.40 2,037.03 1.018 13C12-HXCDF 234 ALT2
0.46 2,284.00 715.21 1,568.79 1.043 13C12-HxCDF 789 ALT1
RO 0.26 0.89 1.053
11,183.55
1.
RO
RO
RO
RO
RO
RO
RO
RO
RO
RO
RO
RO
05-
0.
1.
1.
0.
1.
1.
1.
1.
0.
1.
0.
0.
0.
1.
0.
0.
- ADOVC : njtuur
1.43
64 0.
48 0.
15 8.
88 0.
00 0.
21 56.
23 26.
49 2.
91 5.
16 16.
89
92
26
71
22
17
5 Peaks
DC NL 0
28
29
29
29
29
DC SN 29
DC SN 29
:00
:35
:05
:11
:28
:39
:43
:46
1.
RO
RO
RO
1.
12.
0.
1.
0.
0.
119.
0.950-1.015
78 0.000
56 0.951
05 4.30 3.75 0.955
63 0.962
49 0.965
45 30.92 25.53 0.971
65 14.70 11.95 0.979
60 0.992
08 0.997 123478-HxCDD AN
17 8.67 7.50 1.000 123678-HxCDD AN
01
14
36
86
25
34
46
05-1.43
0.
1.
1.
1.
1.
0.
1.
2.
92
11
22
22
20
77
10
32
5 Peaks
1.
11.
2,448.
2,745.
3,527.
6.
4.
2.
8,738.
19
12
25
61
42
34
63
49
74
6.72 7.32
1.
1.
1.
1.
1.
1.
0.966-
5.84 5.28
1,343.'>8 1,105.17
1,511.31 1,234.30
1,926.48 1,600.94
3.51 4.56
0.
0.
0.
1.
1.
1.
1.
1.
004
010 123789-HxCDD AN PR
014
017
022
023
1.034
000
979
997 13C12-HXCDD 478 STO4
000 13C12-HXCDD 678 IS5
010 13C12-HXCDD 789 RS2
016
018
020
riangle Laboratories, Inc.® Analytical Services Division
D1 Capitals Drive • Durham, North Carolina 27713
hone: (919) 544-5729 • Fax: (919) 544-5491
Printed: 08:19 09/12/97
A
99Q
-------
Page No.
09/12/97
Listing of S975817B.dbf
Matched GC Peaks / Ratio / Ret. Ti»e
Compound/
M_Z.... QC.Log Omit Why ..RT. OK Ratio Total.Area... Area.Peak.1.. Area.Peak. 2. . Rel.RT Compound.Name.. ID.. Flags.
HpCDF
408-410
408-410
13C12-HpCDF
418-420
418-420
HpCDD
424-426
424-426
13C12-HpCDD
436-438
436-436
OCDF
442-444
DC
DC
DC
DC
DC
DC
DC
DC
DC
DC
DC
DC
DC
DC
DC
DC
DC
DC
DC
DC
DC
NL
SN
4
ML
SN
SN
3
ML
SN
SN
WH
WH
2
NL
2
ML
SN
SN
SN
SN
SN
SN
SN
SN
SN
0:00
31:02
31:11
31:23
31:32
32:22
Peaks
0:00
31:10
31:27
32:03
32:22
32:46
Peaks
0:00
31:26
31:38
31:48
32:02
32:16
32:22
Peaks
0:00
31:26
32:01
Peaks
0:00
30:50
31:05
31:18
32:02
32:10
33:40
33:59
34:25
34:40
35:33
0.
RO
RO
RO
0.
RO
RO
RO
RO
0.
RO
RO
RO
RO
0.
RO
RO
0.
RO
RO
RO
RO
RO
RO
RO
RO
RO
-- Aoove:
HXCU1
o /
88-1.20
1
0
0
1
1
1
.47
.32
.99
.02
.30
.03
1
1
73
13
17
20
124
.16
.22
.54
.17
.75
.51
.97
37-0.51
1
0
0
0
0
0
.37
.43
.90
.94
.44
.24
88-1.20
1
1
4
2
1
1
2
.00
.10
.08
.07
.09
.59
.29
1
1,772
4
2
1,215
1
.12
.47
.18
.45
.65
.41
2,992.30
HpCDF /
0
21
0
0
39
0
1
61
.14
.45
.27
.31
.68
.55
.43
.13
88-1.20
1
1
1
.69
.29
.01
76-1.02
0
1
0
2
0
1
1
0
0
0
1
.18
.59
.51
.16
.85
.30
.62
.67
.08
.83
.77
3
5
1,762
.06
.41
.45
1,767.86
HpCDD /
0
1
0
0
0
0
0
1
0
24
1
.17
.49
.59
.36
.87
.70
.85
.38
.42
.70
.15
HpCDF Follows
0.
36.50 Y* 37-°*
6.64 6.53
11.35 , 8.70
10.43* 10.08
0.
535.80 1,236.87
2.60 2.90
370.55 845.10
0.
11.32 10,23
995-1.044
0.
0.
1.
1.
1.
1.
000
996
001 1234 678 -HpCDF
007
012
039 1234789-HpCDF
Ml
UN
936-1.128
0.
1.
1.
1.
1.
1.
000
000 13C12-HpCDF 678
009
028
039 13C12- HpCDF 789
051
XM
SOR5
976-1.006
0.
0.
0.
0.
30.99- 19.02 1.
0.
3.42 2.65
884.29 878.16
Octa-CDD and CDF Follows --
0.
1.
1.
mo
982
988
993
001 1234678-HpCDD
008
Oil
AM
969-1.031
0.
0.
1.
000
982
000 13C13- HpCDD 678
IS7
884-1.116
0.
0.
0.
0.
0.
0.
0.
0.
0.
11.18 13.52 1.
1.
000
893
900
906
928
931
975
984
997
004 OCDF
029
AM
Triangle Laboratories, Inc.® Analytical Services Division
801 Capitola Drive • Durham, North Carolina 27713
Phone: (919) 544-5729 • Fax: (919) 544-5491
Printed: 08:19 09/12/97
230
-------
age No. 6 Listing of S975817B.dbf
9/12/97 Hatched GC Peaks / Ratio / Ret. Time
ompound/
I_Z.... QC.Log Omit Why ..RT. OK Ratio Total.Area... Area.Peak.1.. Area.Peak.2.. Rel.RT Compound.Name.. ID.. Flags.
DC SN 35:52 RO 0.65 1.21 1.039
42-444 1 Peak 24.70
ICDD 0.76-1.02 0.884-1.116
58-460 DC NL 0:00 1.00 0.14 0.000
34:32 0.94 33.29 16.12 17.17 1.000 OCDD Ml
DC SN 34:59 RO 1.25 1.00 1.013
58-460 1 Peak 33.29
.3C12-OCDD 0.76-1.02 0.995-1.005
70-472 DC NL 0:00 RO 1.17 0.11 0.000
34:32 0.79 2,228.58 986.97 1,241.61 1.000 13C12-OCDD IS8
DC WH 34:52 RO 0.36 2.19 1.010
70-472 1 Peak 2,228.58
Description 'Why* Code Description QC Log Desc.
1_Z -Nominal Ion Mass(es) HL-Below Retention Tine Window A-Peak Added
.RT. -Retention Time (nm:ss) WH-Above Retention Time Window K-PeaJc Kept
tat.l -Ratio of M/M+2 Ions SH-Below Signal to Noise Level D-Peak Deleted
)K -RO-Ratio Outside Limits
-------
rile
303.
TRIA
1001
80:
SI)
40:
2n:
o:
rile
305.
TRIA
1001
so:
60:
40:
34J
rile
315.
TRIA
1001
ao:
so:
40:
20.
Tile
317.
TRIA
1001
so:
so:
40:
20:
o:
rile
330.
TRIA
1001
80-
60:
40:
20:
0.
rilt
375.
TRIt
1001
80.
60.
40.
20.
0
tS975B17 tl-848 Adjill-SEP-1997 04:25i31 EI+ Voltage SIR 70S Noises 40
9016 Tt2 BSOB(2S6,3Q,-3.0) PKD(9rS,5,0.05\,160.0,1.00\rr,T) ExptEPCUS
HOLE LABS TextiO-M23-RB TLIH3057 XJKT. TIME - 04:28
M.71S4
A7.50E3 "'I™ ,^'fT 1 I
till i i N 1 i It A1.25X4 A3. 09X4 j
i < tin'' l-3as* 1 f\| I 1 m 1 , U ifl laft f \ L II 1 -/ 1 Hi fc'Vl 1 Ji? S3X3 N - 1 il
JlWS^^JlM
17:00 ' ' 10:00 ' ' 19:00 20tOi
>S975817 41-040 Acqtll-SEP-1997 04t25t31 H+ Voltagm tit 7
8987 Ti2 BSUB(256,30,-3.0) PB>(9,S,5,0 .05\,1513.0;i.00\,r,
NSLE LABS TextsO-H23-RB TLH43057 tK
....
M.«W •"•?•"« J
1JI 3 341T4 at it «*^ 1 • « j»— .^ 1 f
rj^/tvu/'w^ JiAJuUjiA/ W Will
17:00 10:00 15:00 20:00
SS975817 H-848 Acgtll-SEP-1997 04 : 25 1 31 EH- Voltage SIR 7
9419 T:2 BSUB(2S6,30,-3.0) PKD(9,5, 5, 0 .051,188.0,1. 00\,f,l
NGLE LABS TejcttO-M23-RB TLIf43057 IS
Ml. 90
i
17:00 IflloO JiloO 20t««
tS975817 tl-848 Acq ill -SET -1997 04,25*31 XI+ Voltatff SIS 7
9389 Ts2 BSVB(256,30,-3.0) PXD(9,5r5,f. OS\r1332. 0,1. 00\,r,
XGLS LABS Teit.iO-M23-RB TLIt43057 Ut
A2.55
i
17(00 1B\00 19 100 20:00
1S975817 tl-848 Acqtll-SEP-1997 04 : 25 1 31 EH- Voltage SIR 7
9792 r>2 ExpiEPCUS
XSLE LABS Text:O-M23-SB TLH43057 IV
20il6
_£*tjj>.-jlt— 3— *~ — ~^~*rv~~*f~~~^
rf -s-*t~-fj~~ *^
17:00 ' ia»00 1S:00 ' 20»00
:S975817 41-848 Acqill-SEP-1997 04,25,31 XI+ Volttye SIR
8364 F,2 ExpiEPCOS
WGLE LABS TextiO-H23-RB TLI443057 IS
15:57
^uM^LLjM^^^
21:00 ' ' ' 22:00
IS Noise 1 37 8
'; ExptEPCOS
T. TIME - Q4t28
X4
A3.0SJC4 i
*'HlL« **- ill
^ALw« y^^^M^j^/^EM^t
'21:00 ' ' ' '22: 00'
>S Hoi*e,47
SxpiEPCUS
r. THOS - 04,28
V7
'21:00 ' ' ' 22» 00'
IS Soimm:333
f) SxptEPCUS
T. TUB " 04:20
S7
'21:00 ' ' ' '22rOO
IS
T. TIME - 04:20
21 ' *3 -^ J»»Ayv
y«— ^^"
21:00 22:00
IS
T. TIME - 04:20
21:05
^jJLIuJLJyl/^
_r.ir4
.8.9E3
J6-7S3-
.4.5E3
~2-.2Z3
.O.OEO
Time
_i.5r<
_t.2r4
J.QE3
.6.0E3
? or*
" 0 OJffO" '
Ti«e
-4.6E6
.3.7X6
ji.axe
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Ji.OEO
TtMf
-6.1E6
.4.9E6
.3.7X5
_2.STS
.1.2E6
.O.OEO
Time
-1.0E7
.8.0E6
.6.0E6
.4.QE6
-.2.0E6
'•.O.OEO
Time
_I.3r4
i_r.or4
.7.7X3
.5.113
-.2.6X3
.0.0X0
' 17 1 00 ' ' ' 'la'tOO ' ' ' 'is', 00 ' SO1, 00 ' ' '21 100 ' ' .22100' Tim
--
232-
-------
V
rile:S575817 #1-848 Acqsll-SEP-1997 04:25:31 EH- Voltage SIS 70S Holmes 45
319.8965 F:2 BSOB(256,30,-3.0) PKD(7,5, 3,0.05\,180 .0,1.00\,r,T) ElptEPCUS
TRIANGLE LABS TextiO-M23-XB TLI#43057 XK7. TIME - 04:28
1003
aol
so'-
*~
40:
on •
o:
A2.92E4 A1.S8S4
\\\ A3.56E4 A1.90E4 k \ A1.42E4
l\ ^7.22X3 1"'»*oo aotoo aiioo ' ' ' ' aa'ioo' ' ' xtm*
Files S975817 #1-848 Acqill-SEP-1997 04:25:31 XI+ Voltage SIX 70S Nolue,32
321.8936 r:2 BSUB(256,30, -3.0) PKD(7, 5, 3,0. 051,128. 0,1.00\,r,T) ElptEPCUS
TRIANGLE LABS Teit:O-M23-RB TLI#43057 IHJ. TIME - _04s28
100]
80:
60:
—*&.
20:
{ o-
i ~ i/^-» n a v- i-| tfM
°'1^ 'Ll1 ^ nnir)
F A4.30E4 „, ,„„, A1.51I4 1
II ft A2.18E4 . Jl. Al.OOtt A4 43g3
2 SSVB(3S6, 30, -3. 0) PXD(7,S,3,0.05\,124.0,1.00\,r,T) XxptXPCOS
TRIANGLE LABS TBXt:O-M23-KB TLI#43057 UKT. TIME " 04:28
1001
80:
60:
40:
20:
OJ
A2.S1E7
ft
] V
-7.4X6
.5.9X6
.4.4X6
.2.9E6
•JL.5X6
'• o . oxo
19tOO 20:00 2lioO 32\00' ' ' ' Time.
rile:S975817 #1-848 Acqtll-SEP-1997 04:25:31 EI+ Voltage SIX 70S
330.9792 f>2 ExpiEPCUS
TRIANGLE LABS TezttO-M23-XB TLI#43057 IJKT. TIME • 04.28
100]
80:
60:
«o:
20.
o:
21,43 ~^~~»^Sv*nr*
18,19 18^42 _^. ^- sr-^"^^ ~V^ ^f*-~~
-1.0X7
.8.0X6
.6.0X6
.4.0X6
.2.0X6
O.OfO
IStOO 20:00 ' 21^00 ' ' 22\0o' "~ "~ Time
-------
(
V,
FJ.l*:SS7Sei7 tl-848 Acq:ll-SEP-1997 04:25:31 XI+ Voltage SIS 70S Noif*:41
339.8597 T:2 BSOB(256,30,-3.0) PKD(7, 5,3,0. OS\,164 .0,1. 00\,F,T) XxptXPCUS
TRIANGLE LABS Text>O-M23-XB TLI943057 IKT. TIMX - 04:28
J 00*
BOl
60l
40:
20:
0'
A1.29E5
\
A1.24X5 A
1 11
h A1.27X5 A6.50X4 1
(itl *l.03E5 1 1*5.98X4 ,. .,_.
A3.91E4 \\ M k A ft IV 1 A3. 45X4
J\ A5.68E3 A/ I'M" \ J I A /\ J\t\A1'Ji3S4 ll^AS 31f3
f^.1 V A-.—**. A ^_J^VA/^* Y \J ^**^VA_/ \fL^ ^j^VmA/ *VV_ _«Aj *-/ V\-j\ fl VL. nf* M /l/JL* \ f? Aft» */*^ J
.4.2X4
.3.3X4
.2.5X4
.1 . 7X4
.8.3X3
' o . oto
23\00 24\00 ' ' 25tOO ' ' ' 26:00 ' ££*•
TilftS97SB17 tl-848 Acqtll-SEP-1997 04t25>31 XI+ Volt»g» 8Z* 70S Hoimmt281
341.8567 F:2 BSUB(256,30,-3.0) PXD(7 ,5,3,0 .05\, 1124 .0,1. 00\,r,T) XxptXPCUS
TRIANGLE LABS TexttO-M23-SB TLIf 43057 OKT. TIMX " 04:28
100*
aol
60:
40:
At. 36X4
A6.84X4 A8.81X4 15.70E4
1 nft nil )i \ n AJ.«B<
A1.32E4 1 1 Jill MM J U 1 l\ 1
1 ilill I*! 11 1 1 li 111 jia n?r* n
A7 . 06x3 i l/iii /I IfiiJIji ill •••*'•"* II
^i^^.k.^ML^S^ L " WIV UteSP V W ^AMuj^ VSaLi/
-1.7X4
Li . 3X4
Ll . OE4
'•.6.7X3
'.3.4X3
23:00 24:00 25:00 26:00 Time
r±JL»tS975817 tl-848 Acqsll-SEP-1997 04:25:31 EH- Volt»g» SIX 70S Hoiaa:43
351.9000 Tt2 BSUB(256r30,-3.0) PKD(7,5r3,O.OS\,172.0,1.00*,r,T) XxptXPCDS
TRIANGLE LABS T*xttO-K23-XB TLH43057 IKT. TIMX - 04:28
1001
sol
60:
40:
20.
o:
A2.28X7 A3. 27X7
I ft
I
/ V . . J V
^.7.4X6
.5.9X6
.4.4X6
JI.9XS
.1.5X6
• o . oxo
' 23 tOO 24:00 ' ' ' * '2SiOO 26tOo' '..,'?' ' Hmu
rll»tS97S817 tl-848 Acq: 11 -SEP -19 97 04:25i31 XT* Vttltmg* SIX 70S 9oim»>39
353.8970 Jfs2 BSUB(256,30,-3.0) PKD(7,5,3,0.95\t156.0,1.00\,r,T) XxptXPCOS
TXIA1KLX LABS T»xtiO-M23-XB TLH43057 XXX. TIMX - 04:28
10 OS
aol
60:
40:
20:
0:
A1.57E7 AJ..52X7
1 V / v
-4.9X6
.4,0X9
.3.0X6
.2.0X6
.9.9X5
O.OEO
23tOO ' 24\00 25\QO 26\00 T±m»
rile:S975B17 tl-848 Acqtll-SEP-1997 04:25:31 XI+ Voltag* SIX 70S
330.9792 Fi2 XxpiEPCOS
TRIANSLE LABS T*xt.tO-K23-RB TLH43057 TKT. TIME • 04:28
1003
aol
601
40.
20.
0
23-41 23t57 24t20 25:04 ^5t4526^pl^26tl7 , J2!'.50
^yy^v^r^^"*^^^ «^^^vvv*V(r---^-*--V>«^\VV-^-
.1.2X7
.9 . 6X6
.7.2X6
.4.8X6
.2.4X6
o . oro
' 23\00 24tOO' ' ' ' 25\00 26\00 Tim*
rllt:S975B17 tl-848 Acqtll-SEP-1997 04:25:31 XH- Voltage SIX 70S
409.7974 T:2 XxptXPCOS
TRIANGLE LABS T»xttO-M23-XB TLH43057 UKT. TIMX - 04:28
1001
80.
60.
40.
20.
25 15
33.00 «»•»' i 36'13 26t37
22t33 , I 23 i 1 1 2J,5J|"| 34{29 |l |l I a5'54 i 1 Ii
^/MA^^Jl/jAA^A-JrOAJUA^wL^
-2.3X4
.1.8X4
.1.4X4
.9.2X3
.4.6X3
r o.oxo
' 23tOO 24tOO 25iOO 26\00 Ti»«
234
-------
'ile»s375flJ7 #1-848 Acq:ll-SEf-l997 04:25:31 BI+ Volttgm SIX 70S HoimmtSOO
55.8546 T:2 BSUB(256r 30, -3. 0) PXD(7,5,3, 0. 05\,2000.0,1.00\,r,T) ExptSPCOS
TRIANGLE LABS Text:0-M23-XB TLH43057 DKT. TIKE - 04t28
001 A9.21E4
1* , ' i ' 1 i1-""—,' ' ' ~i =*,—-a—, u, 1, i ,—i—,-1 1 • • 'i i
24:00 2StOO 26iOO
File:S975817 #1-848 Acqtll-SEP-1997 04:25:31 EH- Voltage SIX 70S Noif«t37
357.8516 T:2 BSUB(256,30, -3.0) PXD(7,5,3,O.OS\,148.0,1.00\,T,T) ExpiXPCUS
TRIANGLE LABS Text:O-M23-XB TLI#43057 INT. TIME - 04:28
i00*l A5.74E4
so:
60.
40.
20:
A8-*1E4
A8.23E4
25100 26100
Tll*:S975817 #1-848 Acq:ll-SEP-1997 04:25:31 EI+ Voltage SIX 70S No±m»*50
367.8949 Tt2 BSUB(256,30, -3.0) PKD(7,5,3,0.05\,200.0,1.00\,T,T) XxptXPCUS
TRIANGLE LABS Taxt.sO-K23-XB TLH430S7 IXT. TIME - 04i28
lOOi A1.46X7
80J
SO.
40:
20:
~r
-A,
14:00 25100 26:00
rile:S975817 #1-848 Acq:ll-SEP-1997 04i25:31 Eli- Voltage STB 70S Nolaa:35
369.8919 T:2 BSUB(256,30,-3.0) PXD(7,5,3,0.05\,140.0,1.00\,T,T) ExptXPCOS
TRIANGLE LABS T*rt:O-M23-XB TLH43057 IXT. TIME - 04:28
1004 A9.42E6
ao:
601
401
20.
.02X5
24:00 25i00 26:00
rile:S975817 #1-848 Acq:ll-SEP-1997 04:25:31 EI+ Voltage SIS 70S
330.9792 T:2 ExptEPCUS
TXIANGLE LABS T*xt:0-M23-RB TLI#43057 IXT. TIME - 04:28
1001
80.
601
40:
20:
o:
.2.5X4
'.1.9X4
_1. 3X4
.6.3X3
0.0X0
.4.9X6
.3.9X6
.2.9X6
.2.0X6
.9.8X5
0.0X0
Tim,
^3.2X6
.2.6X6
.1.9X6
'.1.3E6
16.4X5
LO.OEO
Tim
.1.2X7
.9.6X6
.7.2X6
.4.8X6
.2.4E6
24:00
25 ,00
2600
.0.0X0
Tim
235
-------
Tile:S975817 #1-406 Acqsll-SSP-1997 04,25,31 EI+ Voltage SIX 70S No±M*:847
373.8208 F:3 BSUB(256,30,-3.0) PXD(7,5,3,0.05*,3388.0,1.00\,r,T) XzptXPCOS
TRIANGLE LABS Text:O-M23-RB TLH43057 UKT. TIMX - 04:28
1004 A3.37E5
27,12 27,24 27:36 27,48 28,00 28,12 28:24 28:36 21,48 39,00 29:12 29:24 29:36 39,48 30,00 30,12
1*,5975817 #1-406 Acqill-SXP-1997 04,25,31 EH- Voltage SIX 70S Soim»,301
375.8178 T,3 BSUBf256,30, -3.0) PB>(7,5,3,0.05\,1204.0,1.00\,T,T) XxptXPCOS
TRIANGLE LABS Teit,O-M23-XB TLH43057 ,JJR7. TIMX - 04:28
1001 A2.69E5 _0
80:
60:
40:
20:
o:
27:12 27,24 27,36 27,48 28:00 28,12 28,24 28,36 28,48 29,00 29,12 29,24 29:36 29:48
rile:SS75817 #1-406 Acq,ll-SXP-1997 04,35,31 EI+ Voltage SIX 70S Bol**,748
383.8639 Tt3 BSUBf 256,30, -3.0) PKD(7,5,3,0.OS\,2992.0,1.Ot\,T,T) XxpiXPCUS
TRIANGLE LABS Text,O-M23-XB TLH43057 Off. TIMX - 04:28
1001 A9.97E6 A9.85X6
Al.82E5
A9.30E4
JU.29X5
A6.33X3
it 171 »-ftr
f.v_.r_w*
^r1^F^TT^^^F^ri*P
A6.04E3
r^rfH
30:00 30:12
ao:
60:
40:
20:
o.
A7.15XS
.9X4
Tim,
.2X4
.4X4
.5X4
.7X4
.8X4
.0X0
M*.
.715
.9E6
.7.
4X3
0X0
27,12 27,24 27,36 27,48 28,00 28:12 28 24 28,3f 38,49 29:00 39:12 39,24 29:36 29,48 30:00 30:12
r±le:S975817 #1-406 Acqill-SXP-1997 04,25,31 XII- Voltage SIX 70S BO±»*,613
385.8610 T,3 BSUB(256,30r-3.0) PKD(7,5,3, 0.051,2452.0,1.00\,r,T) XxptXPCOS
TRIANGLE LABS Toxt:O-H23-SB TLI443057 TXT. TIMX - 04,28
1001 A2.15I7 A3.04X7
80:
60:
40:
20:
A1.57S7
27,12 27,24 27,36 27,48 28,00 28,12 28,24 28:36 28,48 29,00 29,12 29,24 29,36 29:48 30,00 30:12
r±l9,S975817 #1-406 Acq:ll-SEP-1997 04,25,31 XX* Voltag* SIX 70S
392.9760 r,3 XxptXPCOS
TRIANGLE LABS Taxt,O-M23-XB TLI#43057 OKT. TIME - 04,28
7X6
3X6
6X6
1X6
.5X6
0X0
Tlum
27:12 27,24 27,36 27,48 28,00 28,13 38,34 38,36 38,48 39,00 39,13 29,24 29,36 29:48 30:00 30,12
Tilt:3975817 #1-406 Acq,ll-SXP-1997 04,35,31 Eli- Voltage SIX 70S
445.7555 T:3 XzptXPCOS
TRIANGLE LABS T*xt,O-M23-XB TLII43057 IJKT. TIMS • 04,28
27:1227,24 7» 36 27, 4a
28,12 28,24 28,36 28,48 29,00 29,13 29,24 39,36 29,48 30,00 30,12
236
-------
28:00 28:12 ' '28:24 2at36 28:48 29tOO 29>12 29i24 29:36 29i48
rile:S975817 tl-406 Acq:ll-SEP-1997 04*25:31 XI+ Voltage SIX 70S Soifet336
391.8127 F:3 BSUB(256,30, -3.0) PXD(7r5,3,0.05*,1344.0,1.00\er,T) XzpiXPCOS
TXIAWSLX LABS TeztsO-M23-XB TLIt43057 OUT. TIMS - 04i28
>ile:S9758l7 tl-406 Acq:ll-SXP-lS97 04,25,31 EI+ Voltage SIX 70S
89.8156 F:3 BSUB(256,30,-3.0) PXD(7,5,3,O.OS\,8S6.0,1.00\,T,T) ExptSPCUS
TSIASGLX LABS TextsO-H23-XB TLIt43057 IKT. TIME - 04:28
1001 A3.Q9ES
80.
60.
40.
20.
A4.30E4
•f PI*I
27\48
±rfr
A1.47E5
A8.67E4
T
iw A7.11E4
^vA >X
M.42I4
T
"rf
.1.115
'.8.9X4
.6.7X4
'.4.5X4
.2.2X4
0.0X0
Time\
J.UU1
80.
60.
40
20.
^
1
1 1 A1.19X5
I \ A A7.50X4 A7.78X4
A3. 75X4 \ l\ h !\
•\1 ^J \^J V _A ^ ^ V^yv/ V^^'A7!^
^7:48 ' 28^:00 ^ '~28ti2 ' '28:24 '28:36 28\48 29\00 29\12 29t24 29(i36 29t48
.8.0X4
.6.0X4
.4.0X4
.2.0X4
Time
-. — -._
rilesS975817 tl-406 Aoqtll-SXP-1997 04:25,31 XI+ Voltage SIX 70S Soi»e:331
401.8558 Tt3 BSUB(256,30,-3.0) PXD(7,5,3,0.05\t1324.0,1.00\,T,T) XzptXPCOS
TRIANGLE LABS Text:O-M23-XB TLIt43057 HOT. TIMS - 04:28
100S\ Al. 9.3X7
80.
60.
40.
20.
A1.51X7
.6.9X6
.5.5X6
.4.2X6
'.2.8X6
.1.4X6
27:48 28,00 28:12 28:24 28:36 28:48 29:00 29:12 29:24 29:36 29:48
File:S975817 tl-406 Ac
-------
•±la:S975817 tl-430 Acqtll-SEP-1997 04:25:31 EH- Voltagw SJJt 705 Noia»i421
407.7818 T:4 BSUB(256,30,-3.0) PKD(7,5,3,0.05\,1684.0,1.00\,T,T) XxpiXPCUS
TRIANGLE LABS T»It.:O-M23-RB TLH43057 HKT. TIMX - 04:28
10 04 A3.65E5
31:12 31:24 31:36 31:48 33*09 32:12 32:24
rll»:S975817 tl-430 Acq:11-SEP-1397 04:25:31 EI+ Voltagw SIX 70S Holme:283
409.7789 Ft4 BSV3(356r30,-3.0) PXD(7,5,3,0. 05\, 1132.0,1.0t\,T,T) XxpiXPCOS
TRIANGLE LABS Toxt:O-M23-RB TLH43057 ZKT. 11X7 - 04(28
31tl2 31124 31i3S 31:48 32:00 32:12 32:24
r±loiS97S817 H-430 Aoqtll-SEP-1997 04:25:31 11+ Voltiy* SIS 70S Hoi»ut536
417.8253 r:4 BSUS(256,30, -3. 0) PKD(7, 5,3, 0.051,2144.0,1.00\,r,T) ExptEPCOS
TSIASSLE LABS TexttO-M23-SB TLH43057 . OKT. TOO - 04:28
100\ A5.36E6
60:
40:
20:
A6.64E4
A1.13E5
A
A1.04X5
.9.9X4
-7.4E4
.4.9E4
.2.5E4
32:36
33148
0.0X0
T±m>
1001
80:
60:
40.
20:
A3.70E5
OOe=>.
A8.70E4
A1.01E5
-1.3X5
-.1.1X5
-.8.0X4
:.5.4X4
-.2.7X4
io.oxo
32:36
32:40
80J
60:
40:
20:
o
A3. 71X6
.1. 8X6
.1.5X6
JL.1X6
-.7.415
31:12 31:24 31:36 31:48 32,9O 32tl2 32:24
rila>S975817 tl-430 Acqill-SEP-1997 04:25:31 EH- Volttgf SIS 70S Hoi*es392
419.8220 T»4 BSU3(256,30,-3.0) PKD(7,5,3,0 .05\,li6».0,1.00\,T,y) XxptXPCOS
TRIANGLE LABS T*xt:O-M23-RB TLIt43057 UKT. TIME - 04:28
lOOi A1.24E7
32:36
}• a era
32:48 ' Tim*
40:
20:
ol
AS.45X6
-4.3X6
.3.4X6
.2.6Xt
.l.TXf
.8.5X5
0.0X0
31 s 14
31:12 31:24 31:36 31:48 32:00 32:12
Tll»tS975817 tl-430 Aogill-SXP-1997 04:25:31 XI+ Voltagw SIR 70S
430.9729 Ti4 XxptXPCUS
TRIANGLE LABS Ttat:O~H23-RB TLH43057 HK7. TIME
ion
80:
60:
40:
20:
0.
32:24
32:36
32:48
-4.4E6
.3.5X6
.2.6X6
.1. 7X6
.8.7X5
31:12 31:24 31:36 31:48 32:00 32:12 32:24
Tilt:3975817 tl-430 Aoqill-SXP-1997 04:25:31 EI+ Volt*y* SIS 70S
479.7165 Tt4 XxptXPCUS
TRIANGLE LABS TextiO-M23-SB TLH43057 ZK7. TIKE - 04:28
31:08
32:36
32:48
0.0X0
Urn,
31:12
31:24
31136
31:48
32:00
32:12
32:24
32:36
32:48
238
-------
file,S975B17 il-f30 Acqill-SHf-19SrrS4,S'S» 31 B1+ Voltage Six 70S Ubi.eiJS'
423.7766 T:4 BSUB(256,30,-3.0) PXD( 7,5, 3, 0.05\,140.0, 1. 00\,T,T) ExptEPCOS
TRIANGLE LABS TextsO-H23-RB TLH43057 IJKT. TIME - 04,28
100]
so:
eo:
40.
20.
A3. 07X5
\
\
A1.12E5 \
A\
\
/ \ A1.60X4
~~ -~- •"• T ^ r^ ~ ^"~ "^ A r^ ""^nn T
31:18 '31124 JlijO '31t36 '31\42 '31 ',4 8 31,54 'j2i 00 '32\06 '32113 32ilS '32,24 32i30
.6.6X4
.5.3X4
.4.0X4
.2.7X4
-1.3X4
0.0X0
Time
F±le,S975817 tl-430 Acqtll-SXP-1997 04,25,31 EI+ Voltage SIX 70S Holme, 3 5
425.7737 F:4 BSUB(2S6,30,-3.0) PKD(7,5, 3,0 .05\,140 .0, 1.00\,r,T) ExptEFCUS
TRIANGLE LABS TextiO-M23-RB TLH43057 UKT. TIME - 04,28
1001
80.
60:
40.
20:
0.
A1.90E5
}
A1.02E5 1 \
Kl \
\
\
1 \ A7.01K
3 lllB :3l':24 '3l', 30 31i36 '31i42 '31,48 31,54 '32:66 '32t06 32tl2 '32:18 32124 32t30
.5.9X4
.4.7X4
.3.5X4
.2.4X4
.1.2X4
-0.0X0
Time
rile, 3975817 tl-430 Acqtll-SXP-1997 04,25,31 EI+ Voltage SIX 70S Soi*e,1268
435.8169 JTs« BSUB(2S6,30, -3.0) PJO>(7,5,3,0.05\,5073.0,1.00\,F,T) ExptEPCUS
TRIANGLE LABS TexttO-H33-RB TLH43057 UKT. TIME - 04,28
loot
80.
so;
40:
20:
0'
A8.84E6
f\
A
/ V
J \^
31sia '31i24 '31,30 '31:36 '3l>42 '31148 '31,54 32t66 '32\06 32', 12 '32:18 '32:24 '33\30
-2.8X6
.3.3X6
.1.7X6
.1.1X6
.5.6X5
.0.0X0
Time
FiletS975817 tl-430 Aoqtll-SEP-1997 04,25,31 SI+ Voltage SIX 70S Noi*e,750
437.8140 F,4 BSUB(256,30,-3.0) PXD( 7,5,3,0.05%, 3000. 0,1. 00\,r,T) ExpiXPCas
TRIANGLE LABS Text,O-H23-RB TLH43057 XK7. TINE " 04,28
1001
80.
eo:
40:
20:
o:
A8.78E6
f\
A
/ \
j \^
3'l'tie '31:24 31:30 '31:36 '31\42 '31t48 '31:54 '32:66 32:06 '32:12 '32:18 '32:24 '32\30
2.7X6
.2.3X6
.1 . 6X6
.1.1X6
.5.5X5
'0.0X0
Time
Flle:S97S817 tl-430 Aoq:ll-SXP-1997 04,25,31 EI+ Voltage SIX 70S
430.9729 T:4 ExpsEPCUS
TRIANGLE LABS Text I O-M23 -XB TLH43057 JK7. TIME - 04,28
1001
«0_
so:
40.
20.
0.
31:47 31i54 SSiig,^3^^^'
»*&^^tL^^<^^v^^^
3l',18 31:24 31\30 '3l',36 '31\42 '31:48 31i54 J7i 00 32:06 32', 12 32:18 '32*34 32t30
-4.3X6
.3.4X6
.3.6X6
.1 . 7X6
'.8.5X5
0.0X0
Time
230
-------
Ti.leiS975817 tl-430 Acqtll-SEt-1997 04:25:31 XI+ Voltage SIX 70S Koit»>42
41.7428 Fi4 BSU3(256,30,-3.0) FXO( 7,5,3, 0. 05\,168.0,1. 00\,T,T) ExptXPCOS
TRIANGLE LABS Texti!0-H23-RB TLH43057 HOT. TIME • 04*20
31', 00 32'tOO 33tOO 34iOO
rile*S575817 11-430 Aoqill-SXf-1997 04t25i31 XI + Volt*g» SI* 708 Woim»t232
443.7399 Tt4 BSUB(256,30,-3.0) tXD(7,5,3, 0.05%, tit.0,1.00\rf, t) XxptETCUS
TRIANGLE LASS ToxttO-M23-BB TLH43057 ZXT. TZNK - 0412*
1004 A1.35X5
901.
801
701
601
sol
401
35tOO
30J
201
101
I
A7.94Z3
I I -A3^mt
4tmt A6.18E* \ J^-f*^ 1 15 73B | Ih
31:00 32*00 33 i 00 34tOO
rile sSS 7581 7 fl-4JO Acg;ll-srp-1557 04<25tJl rJ*- Volt* ye SXX 70S
430.9729 rs4 XxpiEfCUS
TRIANGLE LABS Text:0-M23-JU> TLH43057 UKT.
35100
TDfS -
100J
50;
80J
70J
601
sol
401
301
201
10!
31t47
31*00 32:00 33*00 34*00
rile*SS75817 #1-430 Acgjll-SJEP-1557 04*25*31 XH- Voltaye SIX 70S
513.6775 t>4 XxptXPCOS
TSIANGLX LABS T*Xt:O-M23-RS TLH43057 IXJT. TIHX -
iOO\
901.
801
701
601
501
40.
30.
20.
10.
0.
32150
34*10
32*01
33*15
04*20
34*50
35
n.
Tim*
.3.5X4
_a.jr<
.a. ow
.1.8E4
'.1.5X4
11.3X4
.1.0X4
.7.6X3
.UC3
.OZ0
-4.4X6
.3.9X6
.3.5X6
.3.1X6
.2.6X6
Ji.ax.6
.1.7X6
.1.3X6
.8.7X5
.4.4X5
.0.0X0
Tim
.8.tC3
31*00
32*00
33*00
34*00
'35*00
240
-------
rU»:sS75817 #1-430 Ac(7,5,3, 0.05\,120.0,1.00\,r,T) ExpiEPCUS
TRIANGLE LABS Tezt:O-M23-SB XLI043057 IJKT. TIHX - 04,28
1001 A1.24E7
34,24 34,30 34,36 34,42 34,48 34', 54
File15S75817 #1-430 Acqtll-SEP-1997 04,25,31 EH- VoltfffU SIX 70S
430.9729 T:4 ExptEPCUS
TXIAHGLX LABS TextiO-M23-SB TLH43057 UKT. TIME - 04,28
1001
80.
60.
40.
20.
0.
35.00
35100
35100
.2.4X4
.1.8E4
.1.2X4
.5.9X3
.0.0X0
Urn,
.1.7X6
-1.4X6
.1.0X6
.5.815
.3.4X5
0.0X0
Time
.2.3X6
.1.8X6
.1.4X6
.9.1X5
.4.6X5
0.0X0
-4.2X6
.3.4X6
.2.5X6
11.7X6
.8.4X5
0.0X0
34,24
34,30
34136
34,42
34:48
34,54
35,00
241
-------
'116:3975817 #1-848 Acq;ll-5fiP-1997 04;25;31 El+ Voltage StR 705
103.9016 F:2 Exp:EPCOS
{ample Text:0-M23-RB TLI#43057
LOOi A3.89E4
INJ. TIME
04:28 File Text:O-M23-RB TLI»
_1.2E4
0 ....
20:00 21:00
?ile:S975817 #1-848 Acq:ll-SEP-1997 04:25:31 EH- Voltage SIR 70S
305.8987 F:2 Exp:EPCOS
Sample Text:0-M23-RB TLI#43057 INJ. TIME -
100%. A6.42E4
22:00
Time
04:28 File Text:O-M23-RB TLI»
_1.5E4
20:00 21:00
File:S975817 #1-848 Acq:ll-SEP-1997 04:25:31 EI+ Voltage SIR 70S
315.9419 F:2 Exp:EPCUS
Sample Text:0-M23-RB TLI#43057 INJ. TIME -
100* 20;21
80J
60J
40J
20 j
22:00
.O.OEO
Time
OJ
04:28 File Text:0-M23-RB TLI>
4.6E6
L3.7E6
L2.8E6
L1.9E6
_9.3B5
20:00
2i!oo
22:00
O.OEO
Time
ro
-------
co ro o -H
H H H H H EH
O 00 •* O
243
-------
•Mle;5975B17 #1-406 Acq;ll-5flP-1997 04.-2S.-31 El+ Voltage SIR 703
189.8156 F:3 Exp:EPCUS
Sample Text:O-M23-RB TLI#43057 INJ. TIME - 04:28 Pile Text:O-M23
LOOi A6.72E4
80J
60J
40J
20J
0
RB TLI»
2.0E4
L1.6E4
11.2E4
L8.2E3
L4.1E3
29:18 29:24 29:30 29:36 29:42 29:48 29:54 30:00 30:06 30:12 30:18 30:24
File:S975817 #1-406 Acq:ll-SEP-1997 04:25:31 EI+ Voltage SIR 70S
391.8127 F:3 Exp:EPCUS
Sample Text:O-M23-RB TLI#43057 INJ. TIME - 04:28 File Text:O-M23
1001 A7.32E4
lO.OEO
Time
RB TLI»
2.5E4
30:12
30:24
29:18 29:24 29:30 29:36 29:42 29:48 29:54 30:00 30i06
File:S975817 #1-406 Acq:ll-SEP-1997 04:25:31 EI+ Voltage SIR 70S
401.8558 F:3 Exp:EPCUS
Sample Text:0-M23-RB TLIU43057 INJ. TIME - 04:28 File Text:O-M23
lOOli 29L28
80J
60J
40j
20 j
OJ
•I'l I I I
29:18
.O.OEO
Time
RD TLI»
6.9E6
L5.5E6
_4.2E6
_2.8E6
_1.4E6
29~l24 29130 29:36
i" i I i i i i i 1 i i
29:42 29:48
i r i "i i i i i i t i
29:54 30»00
30:06 30:12 30:18. 30:24
O.OEO
Time
-------
TLI Project:
Client Sample:
43057
O-M23-RB
Method 23 TCDD/TCDF Analysis (DB-225)
Analysis File: P973847
Client Project:
Sample Matrix:
TLI ID:
Sample Size:
Dry Weight
GC Column:
M23TRAIN
181-27-7AB&*
1.000
n/a
DB-225
Date Received:
Date Extracted:
Date Analyzed:
Dilution Factor
Blank File:
Analyst
08/29/97
09/06/97
09/12/97
n/a
S975807
WK
Spike File:
ICal:
ConCal:
% Moisture:
%Lipid:
% Solids:
SPC2NF04
PF22206
P973843
n/a
n/a
n/a
2,3,7,8-TCDF
ND
0.01
13C,r2,3,7,8-TCDF
13Ca-lA3,4-TCDD
67.7
409&-130%
0.76
0.80
19:41
Quality Control Notes:
* 181-83-1
Dale Received (181-83-1): 09/05/97
Data Reviewer.
09/12/97
Page 1 of 1
Triangle Laboratories, Inc.*
801 Capitola Drive • Durham, North Carolina 27713
Phone: (919) 544-5729 • Fax: (919) 544-5491
Printed: 15:0709/12/97
245
-------
Data Review By:
..Date..
1JU2.
Calculated Nolle Area:
2.07
The Total Area for each peak with an ion abundance ratio outaide
ratio limits has been recalculated according to method requirement*.
Page No.
09/12/97
Listing of P973847B.dbf
Matched GC Peaks / Ratio / Ret. TiM
Compound/
M_Z QC.Log Omit Why ..RT. OK Ratio Total.Area... Area.Peak.1.. Axva.Pttk.2.. Rel.XT Compound.Name.. ID., Flags.
TCDF
304-306
304-306
13C12-TCDF
316-318
316-318
13C12-TCDD
332-334
332-334
DC
DC
DC
DC
DC
DC
DC
DC
DC
DC
DC
DC
DC
NL
SN
SN
SN
SN
SN
0
NL
WL
WL
SN
WH
1
NL
WH
4
0
19
19
19
19
20
-.00
:01
:05
:16
:33
:11
0.
RO
RO
RO
RO
RO
RO
65-0.89
0.95
0
.09
1.12
1.09
0
1
.47
.95
Peaks
0
19
19
20
21
22
:00
:22
:38
:39
:11
:31
0.
RO
1.
0.
0.
0.
0.
0.
0.
96
44
58
60
83
74
00
65-0.89
0
0
0
0
2
0
Peak
0
18
19
19
20
21
:00
:23
:27
:41
:20
:54
0.
RO
RO
RO
.88
.69
.69
.76 2,
.07
.78
2,
2.
9.
13.
170.
3.
18.
170.
Mi*«ne
65-0.89
1
0
0
0
0
2
Peaks
.93
.62
.80 1,
.80 2,
.85
.40
4,
1.
7.
683.
308.
21.
2.
020.
73
53
11
73 937.7*
82
93
73
/•MRf! Vht) 1 MMSB
TdJO FQXXQV*
77
54 3 . 21
09 749.8:
84 1,029.0!
44 9.8:
14
91
1,232.99
0.7M-1.096
0.000
0.921
0.924
0.933
0.947
0.977
0.952-1.048
0.000
0.938
0.9S1
1.000 13C12-2378-
1.026
1.090
TCDT XS«
0.897-1.103
0.000
5.25 0.945
933.26 1.000 13C12-2378-TCDD IS1
1,279.81 1.012 13C12-1234-TCDD RSI
11.62 1.045
1.126
Column Description 'Why* Code Description QC Log Desc.
M_Z -Nominal Ion Maas(es)
..RT. -Retention Tine (mm.-ss)
Rat.l -Ratio of M/M+2 Ions
WL-Below Retention Time Window
WH-Above Retention Time Window
SN-Below Signal to Noise Level
A-Peak Added
K-Peak Kept
D-Peak Deleted
OK -RO-Ratio Outside Limits
-------
fl.J.e,PS7JB47 tl-755 Acqtl2-SEf-i9y7 14*19,22 XI+ Voltago SIX 7OP
303.9016 BSVB(256,30,-3.0) PKD(5,3,1,0.10\,2112.0, 0.00\,T,T) XxptDB225
TRIANGLE LABS Tait:0-H23-RS TLH43057
100\
A8.17X3
20.
17,00 18.00 19,00 20*00 21i00
ttl»iP973847 02-755 Acqtl2-S£P-1997 14>19i22 XX+ Voltigm SIX 7OP Koit»t556
305.8987 BSU3(256,30,-3.0) PKD(5,3,l,0.10\,2224.0,0.00\,r,T) EtpiDB225
TXIAXGLE LABS Text.tO-H23-RB TLH43057
100* A1.27S4
32100
17>00 18,00 19:00 20iOO Sl'tOO
f±10tP973847 tl-755 Acyil2-SXP-1997 14tl9,22 XT* Voltage SIS 7OP Moltmt640
315.9419 BSUB(356,30,-3.0) PlO3(5,3,l,0.10\,2560.0,0.00\,r,r) ExptDB325
TSIAJTSZE LASS TezttO-M23-RB TLH43057
1003k A9.38K6
so:
so:
40:
20:
o:
22100
17>00 18,00 IS,00 20tOO 21,00
r±l*iP973B47 tl-755 Acgtl2-SXP-1997 14tl9,22 XI+ Volt»gm SIX 70P Noli»,727
317.9389 BSUB(2S6,30,-3.0) FKD(S,3,1 f 0.10\,2908. OrO.OO\,r,r> Exp,DB225
TBIJWSLE LASS T»Jct:,O-H23-SS TLI9430S7
1004 A1.23X7
ao:
eo:
40.
20:
sat oo
17:00 18,00 19,00
r±l»tP973847 tl-755 Acq:12-SXP-1997 14,19,22 XH-
375.8364 Exp,DB225
TSIAMGLX LABS T*xtiO-M23-JIB TLH43057
100\
20,00 21:00
SIM 70P
-2.5X6
'.2.0X6
.1.5X6
,1.0X6
.5.1X5
0.0X0
-3.5X6
.3.8X6
.2.1X6
.1.4X6
.6.9X5
0.0X0
17100
18,00
19,00
20,00
21100
22,00
247
-------
T3.1aiP973847 tl-755 Acqil2-SEP-1997 14tl9>22 EI+ VOltfym SIX 70f Koif»>Sia
319.8965 BSVB(256,30,-3.0) PKD(5,3,i, 0.101,2152.0, 0. 00\,T,T) XxpiDB225
TRIANGLE LABS T*xtiO-M23-RS TLH43057
1001
IBiOO 19:00 20i00 21iOO
r±10iP973847 tl-755 Aoqtl2-SXP-1997 14sl9i22 Eli- Voltmgm fit 70P Jtoi««iff08
321.8936 BSUB(256,30,-3.0) PXD(5,3,i, 0.10\,2432.0, 0.00\,r,r) *txpiJ>B225
TRIANGLE LABS TfXttO-H23-SB TLH43057
10D\
22,00
A3.93X3 A4.95X3
A3.37E3 I A5.3SS3
18(00 ISiOO
ril»tP973847 tl-755 Aoqtl2-SXP-1997 14i19i23 XX*
327.8847 BSUB(256, 30, -3.0) PXD(S,3,1, 0.10\,2184.0,0.
TRIANGLE LABS TejrtiO-H23-XB TLIt43057
A1.46I7
80.
60.
40.
20.
18:00 19,00 21:00 21:00
rileiP973847 tl-755 Acqtl2-SEP-1997 14:19:22 EI+ Voltug* SIX 7OP Holaas966
331.9368 BSUB(256,30,-3.Q) PKD(5, 3, 1, 0.10\,3»64 .0,0.00\,T,T) Cxp,DB325
TXIANGLX LABS T*xt,O-M23-SB TLH430S7
1001 A1.03X7
80.
60.
40.
20.
22100
18s 00 IS100 20<00 21<00
Til*tP973847 tl-755 Aoq>12-SEP-1997 14tl9i22 H+ Voltmg* SIX 70P Hoit»t498
333.9338 BSOB(256,30,-3.0) PKD(5,3,1,0.10\,1992.0,0.00\,T,T) SxpiDB225
TRIANGLE LABS TexttO-M23-XB TLH43057
1001 A1.28S7
22:00
80.
60.
40.
20.
0.
A9.33EI
^.4.0X6
,1.6X6
.7.9X5
0.0X0
.2.4X6
'.1. 8X6
.1.2f6
.5.9X5
0.0X0
rim
,.3.7*6
.2.9X6
.2.2X6
J..5X6
.7.3X5
.0.0X0
18(00
19 i 00
20(00
21 «00
22100
O/! O
-------
rilu,P973847 #1-755 Acq,12-SXP-1997 14,19,22
303.9016 Exp,DB225
TRIANGLE LABS TaxtiO-M23-RB TLH43057
1004,
16,52 ,,.*n --;-- 19t
EI+ Voltay* SIS 70f
17,00 is i oo
r±l»,P973847 #1-755 Acq,12-SXP
315.9419 ExpiDB225
TSIAKSLX LABS TmxttO-K23-RB
1001
80.
60.
40:
20:
19,00
1997 14,19,22
TLH43057
20,00
XI+ Valtig* SIS
21,00
22,00
7 OP
o
20 1 39
17,00 18,00 19,00
Tlli,P973847 #1-755 Acqil2-SEP-1997 14,19,22
319.8965 Elp,DB225
TRIANGLE LABS T*xt:0-K23-RB TLH43057
1001 17 45
20,00
EI+ Voltag* SIS
21,00
22,00
70P
17,00 18,00
Tile>P973847 #1-755 Acq,12-SEP
331.9368 Xxp,DB225
TRIANGLE LABS T*xtiO-M23-RB
100)
80:
60:
40l
20:
19,00
1997 14,19,22
TLI943057
20,00
EI+ Volttym SIS
21,00
22,00
70P
17,00 18,00
ril*,P973847 #1-755 Aoq,12-SXP-
292.9825 Exp,DB225
TRIANGLE LABS Text:O-H23-RB
80:
60:
40:
20:
ol
19,00
1997 14,19,22
TLH43057
20,00
SH- Volt»ym SIS
21,00
22,00
70P
17,00 18,00 19,00
rll»,P973847 tl-755 Acq,12-SSP-1997 14,19,22
330.9792 Exp>DB225
TRIANGLE LABS T*XtiO-M23-RB TLH43057
10 0\
20,00
11+ Volt«9» SIS
21,00
22,00
7 OP
.2.0E6
-1.5X6-
.1.0X6
.5.1X5
to.oxo
Tim»
-2.9X6
'•.2.4X6
'-.1.8X6
'•.1.2X6
-.5.9X5
0.0X0
-9.7X6
'•.7.7X6
'•.5.8X6
.3.9X6
.1.9X6
0.0X0
Timm
L 16,55 17,44 18,31 18,56
_.^^£j££~3&j** 31H5 21,55 3a'*3Jt
17,00
18,00
19,00
20,00
-1.1X7
.8.5X6
'•.6.4X6
'•.4.2X6
'•.2.1X6
0.0X0
Tim*
249
-------
Ref. iass 292.9825 Peak top
Height 1,53 volts Span 208 ppi
Systea file naae
Data file naie
Resolution
Group nuaber
lonization aode
Switching
lasses 292.9825,
06225
fl=P973847
292,9825
383,9818
315,9419
317,9389
319,8965
321,8936
327,8847
338,9792
J
K
L
H
1
El*
VOLTAGE.
388.9761
338.S792
331.9368
333,3338
375.8364
Chamel I 3&S792 tektop
Heipj* 1,58 volts Span Mppi
250
-------
,
CALIBRATION
DATA
Triangle Laboratories, Inc.
801 Capitola Drive P.O. Box 13485
Durham, NC 27713-4411 Research Triangle Park, NC 277094483
919-544-5729 Fax # 919-544-5491
251
-------
TRIANGLE LABORATORIES OF RTF, INC.
Initial Calibration Suzanary for PF22206
Date: 02/20/96
Analysis Date : 02/20/96
Instrument : P
Method : C2NF
GC Column...: DB-225
Analytes
2378-TCDF
TOTAL TCDF
2378-TCDD
TOTAL TCDD
RF SD %RSD
1.040 0.109 10%
1.040 0.109 10%
0.992 0.101 10%
0.992 0.101 10%
RT RT/LO RT/HI Ratiol Ratio2 N
21:32 14:31 25:31 0.767
0.767
20:12 16:11 24:11 0.782
0.782
10
10
10
10
Other Standards
37C1-TCDD
RF SD %RSO RT RT/LO RT/HI Ratiol Ratio2 N
1.014 0.048 5% 20:12 18:11 22:11 10
Internal Standards RF SD %RSD RT RT/LO RT/HI Ratiol
13C12-2378-TCDF 1.388 0.062 4% 21:31 20:31 22:31 0.758
13C12-2378-TCDD 1.067 0.03S 3% 20:11 18:11 32:11 0.786
Ratios
N
10
10
Recovery Standards RF SD %RSD
13C12-1234-TCDD 1.000 0.000 0%
RT RT/LO RT/HI Ratiol Ratio2 N
20:27 0.794 10
*•» End of Report
Page
Triangle Laboratories, Inc.® Analytical Services Division
801 Caprtola Drive • Durham, North Carofina 27713
Phone: (919) 544-5729 • Fax: (919) 544-5491
Printed: 23:10 02/20/96
252
-------
TRIANGLE LABORATORIES. INC.
Lai Calibration Summarv for SF5;11~
Dot*. 06/10/97
naiysis Date. . . . :
.nalytes
'otal MCDF
'otal MCDD
'otal 3CDF
'otal CCDD
•otal TriCDF
Jotal TriCDD
J378-TCDF
IOTAL TCDF
!378-TCDD
JOTAL TCDD
.2378-?eCDF
!3 47 8 -PeCDF
:OTAL PeCDF
L2378-?eCDD
TOTAL PeCDD
L23478-a3eCDF
123678-HxCDF
234678-HxCDF
L23789- HxCDF
TOTAL HxCDF
123478-HxCDD
123678-HxCDD
123789-axCDD
COTAL HxCDD
1234678-HpCDF
1234789-HpCDF
TOTAL HpCDF
1234678-HpCDD
TOTAL HpCDD
XDF
3CDD
3ther Standards
37C1-TC3D
13C12-?eCDF 234
13C12-HXCDF 478
13C12-3XCDF 234
13C12-3XCDF 789
13C12-HXCDD 478
L3C12-3pCDF 789
Internal Standards
13C12- 2378 -TCDF
13C12-2378-TCDD
13C12- PeCDF 123
OS/'O/Q?
3
2
1
0
1
1
0
1
1
1
1
1
1
1
1
1
1
1
1
1
1
0
1
1
1
1
1
1
1
1
1
1
SF
.087
.525
.587
.326
.082
.933
.251
.251
.191
.191
.111
.115
.113
.256
.256
.215
.574
.247
.105
.285
.953
.133
.091
.059
.543
.184
.363
.068
.068
.493
.105
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
RF
0
0
0
0
0
0
0
.843
.970
.959
.926
.805
.973
.771
0
0
0
0
0
0
0
RF
1
1
1
.318
.066
.133
0
0
0
so
.000
.000
.000
.000
.000
.000
.116
.116
.231
.231
.082
.061
.069
.113
.113
.064
.099
.069
.060
.062
.067
.070
.067
.067
.103
.100
.095
.089
.089
.131
.066
SO
.038
.030
.042
.021
.044
.027
.049
3D
.065
.020
.051
*RSD
0%
0%
0%
0%
0%
0%
9%
9%
19%
19%
7%
5%
6%
9%
9%
5%
6%
6%
5%
5%
7%
6%
6%
6%
7%
8%
7%
8%
8%
9%
6%
%RSD
5%
3%
4%
2%
5%
3%
6%
%RSD
5%
2%
5%
Page
M«r *\nri . . . .
RT
8:15
8:42
10:38
11:09
13:59
14:03
19:43
20:36
24:12
24:59
25:22
27:55
28:01
28:32
29:15
28:41
28:46
29:03
30:45
31:57
31:37
34:09
34:03
RT
20:36
24:58
27:55
28:32
29:15
28:40
31:57
RT
19:43
20:34
24:11
1
RT/LO
0:01
0:34
6:43
7:34
10:43
12:34
15:43
16:34
20:11
21:21
24:01
24:45
26:45
27:36
30:02
30:02
RT/LO
18:34
22:11
28:45
RT/LO
18:43
18:34
20:11
Ki
3 :
4:
t :
• 3 ;
IT:
19:
23:
24:
23:
29:
32:
32:
34:
35:
38:
38:
- y
HI
43
34
43
34
43
34
43
34
11
21
01
45
45
36
02
02
RT/HI
22:
26:
34:
34
11
45
RT/HI
20:
22:
28:
43
34
11
T? "*
Ratiol Ratio2
;
2
5
2,
i
T
0
0
0
0
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
0
0
0
0
.931
.327
.965
.609
.025
.064
.799
.799
.772
.772
.552
.470
.509
.526
.526
.247
.260
.243
.246
.249
.265
.251
.233
.249
.034
.080
.053
.993
.993
.876
.902
Ratiol Ratio 2
1
0
0
0
1
0
.470
.518
.517
.519
.241
.424
Ratiol Ratio 2
0
0
1
.734
.802
.447
S
1
1
1
1
1
1
5
5
5
5
5
5
5
5
5
5
5
5
5
5
5
5
5
5
5
5
5
5
5
5
5
5
5
5
5
5
5
5
N
5
5
5
langle Laboratories, Inc.® Analytical Services Division
11 Capitola Drive • Durham, North Carolina 27713
lone: (919) 544-5729 • Fax: (919) 544-5491
Printed: 09:49 06/10/97
253
-------
TRIANGLE LABORATORIES. INC. Date: 06/10/9?
Initial Calibration Summary for srS6117
13C12-PeCDD 123 0.535 0.082 13% 25:21 21:21 29:21
13C-.2-HXCDF 678 l.:04 0.073 6% 28:01 24:01 32:01
13C12-HXCDD 678 0.995 0.017 2% 28:45 27:45 29:45
13C12-HpCDF 678 0.387 0.046 5% 30:45 28:45 34:45
13C12-HpCDD 678 0.315 0.077 9% 31:36 30:36 32:36 .019 5
13C12-OCDD 0.519 0.080 15% 34:02 32:02 36:02 :.366 5
461 S
522 :
240 5
429 5
Recovery Standards RF SD %RSD RT RT/LO RT/HI Retiol Ratio2 M
13C12-1234-TCDD 1.000 0.000 0% 20:21 0.811 S
13C12-HXCDD 789 1.0000.000 0% 29:02 ', .1.231 5
••• End of Report **»
Page
Triangle Laboratories, Inc.® Analytical Services Division
801 Capitals Drive • Durham, North Carolina 27713 Printed: 09:49 06/10/97
Phone: (919) 544-5729 • Fax: (919) 544-5491
-------
Dac«: 34/09/9V
cali&racion sunnaur/ lor XF24Q87
aalysis Daca : 04/08/97
CC
: CZSF
. . : BB-22S
378-TC3F
OTJU. TOff
378-TCXD
11 'ID
Standards
L3G2-2378-1K3D
wy St
L3C2-U34-1C3D
HP SO UtSO
0.967 0.044 5%
0.967 0.044 5%
1.095 0.097 9%
1.095 0.09? 9%
3S SO %8SD
1.018 0.047 5*
H? 9 1BSD
1.392 0.071 5%
1.105 0.037 3*
a? so
1.000 o.ooo
RT RT/LO BT/BZ Baelel 3mc±o2 V
21:49 14:49 25:49 0.779 10
0.779 10
20:37 16:36 24:36 0.793 10
0.793 10
RT BT/IiO BT/BZ P»*~*al Raring y
20:37 18:36 22:36 10
RT BS/LO BT/BZ BmeioJL 3*cio2 H
21:49 20:49 22:49 0.787 10
20:36 18:36 22:36 0.783 10
0%
RT BT/LO BT/BZ HmCiol
20:50 0.796 10
• Ouham. North Cvoin 27713
ttorw (919) 544-5729 • Ptac (919) 544-5491
PimM: 02:46 04/09/97
-------
Date: 09/12.-9" TRIANGLE LABORATORIES OF RTr. ::~.
Continuing Calibration for ??72343
Analysis Data : 09/12/97 Methci
Operator : WK
Init Calibration.: PF22206
ICal Date : 02/20/96
Analysis Time....: 11:04
Instr^r.er.z. . : P
Std.C;r.c ---- : 5.00
GC Cclvair....: D3-225
Analyte Suiranary
Name
2378-TCDF
TOTAL TCDF
2378-TCDD
TOTAL TCDD
RF Ratio
RT
ICal 0*1 ta
RT Rel. RT RF RF %D
1&2 Lo/High
0.964 0.76 16:14 20:40 1.0008 1.040 -0.076 -7.3%
22:38
0.964 0.76 1.040 ,-0.076 -7.3%
1.001 0.75 17:03 19:28 1.0009 0.992 0.009 0.9%
22:00
1.001 0.75 0.9»2 0.009 0.9%
Other Standard Summary ICal Delta
Name RF Ratio RT RT Rel. RT RF RF %D
It2 Lo/High
37C1-TCDD 0.937 17:27 19:28 1.0009 1.014 -0.077 -7.6%
21:27
Internal Standard Summary ICal Delta
Name RF Ratio RT RT B»l. KT RF 8P %D
162 Lo/High
13C12-2378-TCDF 1.201 0.77 19:39 20:39 1.0000 1.38S -0.187 -13.5%
21:39
13C12-2378-TCDD 1.006 0.79 17:27 19:27 1.0000 1.067 -0.061 -5.7%
21:27
Recovery Standard Summary ICal Delta
Name RF Ratio RT RT Rel. RT RF RF %D
1&2 Lo/High
13C12-1234-TCDD 1.000 0.82 19:41 1.0120 1.000 0.000 0.0%
Page
Triangle Laboratories, Inc.® Analytical Services Division
801 Caprtola Drive • Durham, North Carolina 27713
Phone: (919) 544-5729 • Fax: (919) 544-5491
Printed: 11:46 09/12/97
-------
Date 3/10/r-
lnai'.*£*5 Date
^naiy'e Summary
teme
Total MCDF
Total MCDD
Total DCDF
Total DCDD
Total TriCDF
Total TriCDD
2378-TCDF
TOTAL TCDF
2378-TCDD
TOTAL TCDD
12378-PeCDF
23478-PeCDF
TOTAL PeCDF
12378- PeCDD
TOTAL PeCDD
123478 -HxCDF
123678 -HxCDF
234678 -HxCDF
123789-HxCDF
TOTAL HxCDF
123478-HxCDD
TRIANGLE LABORATORIES. INC.
Continuinu Calibration for S975
• 09/10/97 Method
. - . i J / i. w/ * i
. . : BJG
-. . : SF56117
• 06/10/97
RF Ratio
U2
0.000
0.000
0.
0.
0.
0.
1.
1.
1.
1.
1.
1.
1.
1.
1.
0.
1.
0.
0.
1.
0.
000
000
000
000
150
150
191
191
091
133
112
229
229
997
240
966
889
023
942
~ "
Instrument . .
Std.Conc. . .
ST RT Rel. RT
Lo/High
0:23
14:23
1:12
15:
12
7:23
15:
23
8:12
0
0
0
0
1
1
1
1
1
1
1
1
1
1
1
.81
.81
.78
.78
.54
.52
.53
.58
.58
.25
.26
.28
.26
.26
.21
16:
11:
18:
13:
19:
16:
22:
18:
22:
22:
26:
23:
26:
27:
29:
12
23
23
12
12
46 20:24 1.0008
30
10 21:13 1.0008
30
27 24:43 1.0007
39
25:29 1.0317
48 25:52 1.0006
31
13 28:22 0.9971
57
28:28 1.0006
28:59 1.0187
29:42 1.0439
27:45 29:07 0.9977
• M2 :-T
: S
ICal
SF
2.087
1.625
0.
1.
1.
0.
1.
1.
1.
1.
1.
1.
1.
1.
1.
1.
1.
1.
1.
1.
687
326
082
933
251
251
191
191
111
115
113
256
256
215
574
247
105
.285
0.953
50.00.
Delta
RF
-2.087
-1.625
-0
-1
-1
•
-0
-0
-0
0
0
-0
0
-0
-0
-0
-0
-0
-0
-0
-0
-0
.687
.326
.082
.933
.101
.101
.000
.000
.020
.018
.001
.027
.027
.218
.334
.281
.216
.262
.011
%D
100.0%
100.0%
100.0%
100.0%
100.0%
100.0%
-8.1%
-8.1%
0.0%
0.0%
-1.8%
1.7%
-0.1%
-2.2%
-2.2%
-17.9%
-21.2%
-22.5%
-19.6%
-20.4%
-1.1%
29:38
123678-HxCDD
1.
,080
1
.20
29:12 1.0006
1,
.133
-0
.053
-4.7%
Page
'riangle Laboratories, Inc.® Analytical Services Division
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Printed: 14:20 09/10/97
. 257
-------
123 • = •»- HxCDD
rOT.-.l HxCDD
1234b^8-HpCDF
1234789-HpCDF
TOTAL HpCDF
1234678- HpCDD
TOTAL HpCDD
OCDF
OCDD
1
1
1
1
1
0
0
1
1
(.
.062
.028
.504
.157
.331
.992
.992
.433
.042
.ontinui
1.20
1.08
1.06
1.07
1.01
1.01
'0.93
0.84
.no Ca-.z:
31:. 1
32:34
31:1-
32:13
30:30
38:30
30:30
38:30
~3~-
* i? •
31:
32 :
32:
34:
34:
~
; j
23
02
38
31
:or Sir ;
1.0105
1.0000
1.0390
1.0000
1.0039
1.0005
Other Standard Summary
Name
37C1-TCDD
13C12-PeCDF 234
13C12-HXCDF 478
13C12-HXCDF 234
13C12-HXCDF 789
13C12- HxCDD 478
13C12- HpCDF 789
Internal Standard
Name
13C12-2378-TCDF
13C12-2378-TCDD
13C12-PeCDF 123
13C12-PeCDD 123
13C12-HXCDF 678
13C12- HxCDD 678
0
0
0
0
0
1
0
RF
.955
.992
.982
.906
.776
.010
.811
Ratio
162
1.47
0.46
0.47
0.44
1.20
0.42
RT
Lo/High
19:12
23:12
20:42
28:42
29:10
35:10
RT
21:
25:
28:
28:
29:
29:
32:
13
28
21
58
41
06
22
Rel. RT
1.0008
1.0310
0.9965
1 . 0182
1.0434
0.9971
1.0385
Summary
1
1
1
0
1
0
RF
.464
.086
.228
.746
.243
.970
Ratio
IS, 2
0.76
0.81
1.44
1.51
0.47
1.20
RT
Lo/Hi?h
19:23
21:23
19:12
23:12
20:42
28:42
21:51
29:51
24:27
32:27
28:11
30:11
Page
RT
20:
21:
24:
25:
28:
29:
2
23
12
42
51
27
11
Rel. RT
1.0000
1.0000
1.0000
1.0000
1.0000
1.0000
••?7
1.091
1.059
1.543
1.184
1.363
1.068
1.068
1.493
1.105
ICal
RF
0.843
0.970
0.959
0.92E
0.805
0.973
0.771
ICal
RF
1.318
1.066
1.133
0.635
1.204
0.995
- .'.029
-,.031
-J.039
- 5.027
- J.032
-J.076
-0.076
-0.060
-0.063
Delta
RF
0.112
0.022
0.023
-0.020
-O.029
0.037
0.040
2*1 ta
RF
0.146
0.020
0.095
0.111
0.039
-0.025
-2
-2
-2
_2
-2
-7
-7
-4
-5
%D
13
2
2
-2
-3
3
5
%D
11
1
8
17
3
-2
.5%
.9%
.5%
.3%
.4%
. 1%
.1%
.0%
.7%
.2%
.3%
.4%
.1*
.7%
.8%
.2%
.1%
.9%
.4%
.6%
.3%
.5%
Triangle Laboratories, Inc.® Analytical Services Division
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Printed: 14:20 09/10/97
258
-------
ice: 09/ll>/37
Continj.
iC12-HpCDF S78 u."0 0.44
iC12-HpCDD =78 0."3S 1.02
IC12-OCDD 0.446 0.89
scovery Standard S
ime S" Ratio
1&2
5C12-1234-TCDD 1. JOO 0.80
IC12-HxCDD 789
1.000 1.22
!£ LABORATORIES. ISC.
.-.J Calibration for 5975797
29:1C 31:10 i.::00 0.887 -0.137 -15.5%
35 :1C
31:02 32:02 1.1000 0.815 -0.029 -2.5%
33:0:
34:21 34:30 1.0000 0.519 -0.073 -14.0*
34:41
ICal Delta
RT RT Rel. RT RF RF %D
lo/Hich
20:59 0.9898 1.000 0.000 0.0%
29:29 1.0103 1.000 0.000 0.0%
QC Front End Check:
1.5494
Page
iangle Laboratories, Inc.® Analytical Services Division
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Printed: 14:20 09/10/97
259
-------
Date: 09/11/97
TRIANGLE LABORATORIES, INC.
Continuing Calibration for S975814
Operator
• JM
Init Calibration.: SFSS117
ICal Date
Analyte Summary
Name
Total MCDF
Total MCDD
Total DCDF
Total DCDD
Total TriCDF
Total TriCDD
2378-TCDF
TOTAL TCDF
2378-TCDD
TOTAL TCDD
12378-PeCDF
23478-PeCDF
TOTAL PeCDF
12378 -PeCDD
TOTAL PeCDD
123478-HxCDF
123678-HxCDF
234678-HxCDF
123789-HxCDF
TOTAL HXCDF
123478 -HxCDD
123678 -HxCDD
• 06/10/97
RF Ratio
1&2
0.000
0.000
0.000
0.000
0
0
1
1
1
1
1
1
1
1
1
1
1
1
0
1
0
1
.000
.000
.118
.118
.146
.146
.093
.143
.118
.209
.209
.097
.379
.073
.977
.132
.855
.058
0.80
0.80
0.80
0.80
1.53
1.50
1.51
1.59
1.59
1.28
1.29
1.27
1.29
1.28
1.23
1.24
Instrument* -
Std.Conc
Related C
RT RT Rel. RT
Lo/High
0:24
14:24
1:13
15:13
7:24
15:24
8:13
16:13
11:24
18:24
13:13
19:13
16:44 20:25 1.0008
22:28
18:06 21:14 1.0008
22:28
. : S
50.00
ICal: S975778
ICal
RF
2.087
1.625
0.687
1.326
1
0
1
1
1
.082
.933
.251
.251
.191
1.1S1
22:24 24:43 1.0007
26:38
25:29 1.0317
23:47 25:52 1.0013
26:30
27:11 28:22 0.9965
29:56
28:28 1.0000
28:59 1.0181
29:41 1.0427
27:44 29:07 0.9977
29:37
29:12 1.0006
Page 1
1
1
1
1
1
1
1
1
1
1
0
1
-111
.115
.113
.256
.256
.215
.574
.247
.105
.285
.953
.133
Delta
RF
-2.087
-1.625
-0.687
-1.326
-1
-0
-0
-0
-0
-0
-0
0
0
-0
-0
-0
-0
-0
-0
-0
-0
-0
.082
.933
.133
.133
.045
.045
.018
.028
.005
.047
.047
.118
.195
.174
.128
.153
.098
.075
%D
100.
100.
100.
100.
100.
100.
-10.
-10.
-3.
0%
0%
0%
0%
0%
0%
6%
6%
8%
-3.8%
-1.
2.
0.
-3.
-3.
-9.
-12.
-13.
-11.
-11.
-10.
-6.
6%
5%
5%
7%
7%
7%
4%
9%
6%
9%
3%
6%
Triangle Laboratories, Inc.® Analytical Services Division
801 Capitola Drive • Durham, North Carolina 27713
Phone: (919) 544-5729 • Fax: (919) 544-5491
Printed: 03:04 09/11/97
2RO
-------
ie: 09/11/97
TRIANGLE LABORATORIES.
Continuing Calibration
3789 -HxCDD
TAL HxCDD
34678-HpCDF
34789 -HpCDF
TAL HpCDF
34678-HpCDD
TAL HpCDD
DF
DD
her Standard
me
Cl-TCDD
C12-PeCDF 234
C12-HXCDF 478
C12-HXCDF 234
C12-HXCDF 789
C12-HXCDD 478
C12- HpCDF 789
1.052
0.989
1.384
1.094
1.239
1.001
1.001
1.470
1.049
Summary
RF
0.972
1.014
0.955
0.886
0.798
0.897
0.787
1.24
1.24
1.04
1.05
1.04
1.03
1.03
0.88
0.90
Ratio
1&2
1.54
0.50
0.49
0.49
1.22
0.43
31:01
32:33
31:16
32:13
30:32
38:32
30:32
38:32
RT
Lo/High
19:13
23:13
20:42
28:42
29:11
35:11
29:
31:
32:
32:
34:
34:
RT
21:
25:
28:
28:
29:
29:
32:
29
11
23
03
39
32
INC.
for S975314
1
1
1
1
1
1
.0103
.0000
.0385
.0005
.0034
.0000
Rel. RT
13
28
21
58
41
06
22
1
1
0
1
1
0
1
.0000
.0310
.9959
.0176
.0427
.9971
.0379
ternal Standard Summary
me
C12-2378-TCDF
C12-2378-TCDD
C12-PeCDF 123
212-PeCDD 123
C12-HxCDF 678
C12- HxCDD 678
RF
1.554
1.110
1.243
0.713
1.294
0.964
Ratio
162
0.74
0.78
1.52
1.58
0.50
1.22
RT
Lo/High
19:24
21:24
19:13
23:13
20:42
28:42
21:50
29:50
24:28
32:28
28:11
30:11
Page
RT
20:
21:
24:
25:
28:
29:
2
24
13
42
50
28
11
Rel. RT
1
1
1
1
1
1
.0000
.0000
.0000
.0000
.0000
.0000
1.091
1.059
1.543
1.184
1.363
1.068
1.068
1.493
1.105
ICal
RF
0.843
0.970
0.959
0.926
0.805
0.973
0.771
ICal
RF
1.318
1.066
1.133
0.635
1.204
0.995
-0.039
-0.070
-0.159
-0.090
-0.124
-0.067
-0.067
-0.023
-0.056
Delta
RF
0.129
0.044
-0.004
-0.040
-0.007
-0.076
0.016
Delta
RF
0.236
0.044
0.110
0.078
0.090
-0.031
-3.
-6.
-10.
-7.
-9.
-6.
-6.
-1.
-5.
%D
15.
4.
-0.
-4.
-0.
-7.
2.
%D
17.
4.
9.
12.
7.
-3.
5%
7%
3%
6%
1%
3%
3%
5%
1%
3%
5%
4%
3%
8%
8%
1%
9%
2%
7%
3%
5%
1%
ingle Laboratories, Inc.® Analytical Services Division
Capitola Drive • Durham, North Carolina 27713
>ne: (919) 544-5729 • Fax: (919) 544-5491
Printed: 03:04 09/11/97
9R1
-------
D*te: 09/11/97 TRIANGLE LABORATORIES, INC.
Continuing Calibration for S575814
13C12-HpCDF 678 0.876 0.45 29:11 31:11 1.0000 0.887 -0.011 -1.3%
35:11
31:02 32:02 1.0000 0.815 -0.033 -4.1%
33:02
34:22 34:32 1.0000 0.519 -0.085 -16.3%
34:42
13C12-HpCDD 678 0.782 1.06
13C12-OCDD 0.434 0.84
Recovery Standard Summary
Name RF Ratio
RT
ICal Delta
RT Rel. RT RP RF
%D
162 Lo/High
13C12-1234-TCDD 1.000 0.83
13C12-HxCDD 789 1.000 1.22
21:00 0.9898 1.000.^0.000 0.0%
29:29 1.0103 1.000 0.000 0.0%
QC Front End Check:
1.6171
Page
Triangle Laboratories, Inc.® Analytical Services Division
801 Capitola Drive • Durham, North Carolina 27713
Phone: (919) 544-5729 • Fax: (919) 544-5491
Printed: 03:04 09/11/97
-------
Date: 09.11/9"
TRIANGLE LABORATORIES. 2IC.
Continuing Calibration Jcr X973069
Analysis Date : 09/11/97
Operator : 3JG
Init Calibration.: XF24087
ICal Dace : 04/08/97
Analysis Time : 12:00
Method : C2NF
Instrument..: X
Sti.Conc : 5.:o
GC Column...: DB-225
Analyte Summary
Name
2378-TCDF
TOTAL TCDF
2378-TCDD
TOTAL TCDD
ICal Delta
RF Ratio RT RT Rel. RT RF RF %D
1&2 Lo/High
1.051 0.81 17:54 22:29 1.0015 0.967 0.084 8.7%
24:42
0.967 0.084 8.7%
1.051 0.81
1.079 0.78
1.079 0.78
18:43 21:12 1.0016 1.095 -0.016 -1.4%
23:58
1.095 -0.016 -1.4%
Other Standard Summary ICal Delta
Name RF Ratio RT RT Rel. RT RF RF %D
1&2 Lo/High
37C1-TCDD 0.967 19:10 21:12 1.0016 1.018 -0.051 -5.0%
23:10
Internal Standard Summary ICal Delta
Name RF Ratio RT RT Rel. RT RF RF %D
1&2 Lo/High
13C12-2378-TCDF 1.285 0.80 21:27 22:27 1.0000 1.392 -0.107 -7.7%
23:27
13C12-2378-TCDD 1.000 0.78 19:10 21:10 1.0000 1.105 -0.105 -9.5%
23:10
Recovery Standard Summary ICal Delta
Name RF Ratio RT RT Rel. RT RF RF %D •
1&2 Lo/High
13C12-1234-TCDD 1.000 0.78 21:27 1.0134 1.000 0.000 0.0%
Page
Triangle Laboratories, Inc.® Analytical Services Division
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Printed: 13:18 09/11/97
-------
CASE NARRATIVE
Analysis of Samples for the Presence of
Polychlorinated Dibenzo-p-Dioxins and Dibenzofurans by
High-Resolution Chromatography / High-Resomtkm Mass Spectrometry
Method 23 (6/93)
Date:
Client ID:
P.O. Number:
TLI Project Number:
September 11,1997
Pacific Environmental Services
104-98-0019 & -0020
43057rl
This report should only be reproduced in full. Any partial reproduction of this report requires permission from
Triangle Laboratories, Inc.
Rev. 05/08/97
Triangle Laboratories, Inc.
801 Cap/to/a Drive P.O. Box 13485
Durham, NC 27713-4411 Research Triangle Park, NC 27709-3485
919-544-5729 Fax # 919-544-5491 \
-------
Triangle Laboratories, Inc. September 11,1997
Case Narrative 43057rl
Overview
Seven M23 samples were received from Pacific Environmental Services in good condition
on August 29,1997 at 19 °C. One XAD trap for sample O-M23-RB was received from
Pacific Environmental Services without a chain-of-custody in good condition on
September 5,1997 at ambient temperature. The samples were stored in a refrigerator at
4°C until the time of extraction. The M23 samples and associated QC sample were
extracted and analyzed according to procedures described in the Triangle Laboratories'
Data User's Manual (Rev. 12/92-HK-2-AH-2/93). Any particular difficulties encountered
during the samples' handling by Triangle Laboratories will be discussed in the QC
Remarks section below. Results reported relate only to the items tested.
Quality Control Samples
A laboratory method blank, identified as the TLIM23 Blank, was prepared along with the
samples.
Quality Control Remarks
This release of this particular set of Pacific Environmental Services analytical data by
Triangle Laboratories was authorized by the Quality Control Chemist who has reviewed
each sample data package individually following a series of inspections/reviews. When
applicable, general deviations from acceptable QC requirements are identified below and
comments are made on the effect of these deviations upon the validity and reliability of the
results. Please consult Triangle Laboratories' Data User's Manual for further details.
Specific QC issues associated with this particular project are:
Sample Preparation Laboratory: None
Mass Spectrometry: The archived extracts of samples O-M23-4 and the method blank
were processed through normal cleanup procedures because sample O-M23-4 was
destroyed in the wet laboratory during filtration.
Data Review: None
Other Comments: Any analytes found in the TLI M23 Blank are detected at a level equal
to or less than the Target Detection Limit. This level of contamination is acceptable as per
TLI guidelines.
-------
Triangle Laboratories, Inc. September 11,1997
Case Narrative 43057rl
Sample Calculations:
Analyte Concentration
The amount of any analyte is calculated using the following expression.
Ao* Qp
Amt (a)= —
AP*RRF(
-------
Triangle Laboratories, Inc. September 11,1997
Case Narrative 43057rl
DL(0) is the estimated detection limit for a target analyte,
2.5 is the minimum response required for a GC signal,
F is an empirical number that approximates the area to height ratio for a GC signal. This
number is 3.7 for both the DB-5 GC column and the DB-225 GC column,
H is the height of the noise
Ap is the integrated current of the characteristic ions of the corresponding internal
standard,
Qp represents the amount of internal standard added to the sample before extraction,
RRF(a) is the mean analyte relative response factor from the initial calibration (ICal) and,
W is the sample weight or volume
The detection limit is expressed in nanograms (ng) or picograms (pg).
Other sample calculations may be found in the Triangle Laboratories Data User's Manual.
Data Flags
In order to assist with data interpretation, data qualifier flags are used on the final reports,
as discussed in Triangle Laboratories' Method 23 Data User's Manual. Please note that all
data qualifier flags are subjective and are applied as consistently as possible. Each flag has
been reviewed by two independent Chemists and the impact of the data qualifier flag on
the quality of the data discussed above. The most commonly used flags are:
A 'B' flag is used to indicate that an analyte has been detected in the laboratory method
blank as well as in an associated field sample. The 'B' flag will be used only when the
concentration of analyte found in the sample is less than 20 times that found in the
associated blank. This flag denotes possible contribution of background laboratory
contamination to the concentration or amount of that analyte detected in the field sample.
Under Triangle Laboratories guidelines, a laboratory blank is acceptable if the tetra-
through hepta-CDD/CDF levels are all below the target detection limits (TDLS) or if the
contamination levels are less than 5% of the levels detected in the associated field samples.
If these conditions are satisfied or if the blank is unable to be reextracted, the
interpretation of the contamination levels relative to the samples should be as follows: 1)
analyte quantitations should be considered valid if the level of blank contamination is less
than five percent of the level detected in the field sample, 2) analyte quantitations should
-------
Triangle Laboratories, Inc. September 11,1997
Case Narrative 43057r1
be considered estimated if the analyte level in the sample is five to twenty times the level
of the analyte in the blank, or 3) analytes whose level in a sample is the same as or less
than five times the level detected in the associated blank should be considered present
likely due to laboratory contamination and not native to the sample.
An 'E' flag is used to indicate that an PCDF peak has eluted at the same time as the
associated diphenyl ether (DPE) and that the DPE peak intensity is ten percent or more of
the PCDF peak intensity. Total PCDF values are flagged 'E' if the total DPE contribution
to the total PCDF value is greater than ten percent All PCDF peaks that are significantly
influenced by the presence of DPE peaks are quantitated with EMPC values, regardless of
the isotopic abundance ratio. These EMPC values are most likely overestimated due to
the DPE contribution to the peak area.
An T flag is used to indicate labeled standards have been interfered with on the GC
column by coeluting, interferent peaks. The interference may have caused the standard's
area to be overestimated. All quantitations relative to this standard, therefore, may be
underestimated.
A 'PR' flag is used to indicate that a GC peak is poorly resolved. This resolution problem
may be seen as two closely eluting peaks witboota reasonable valley between the peak
tops, overly broad peaks, or peaks whose shapes vary greatly from a normal distribution.
The concentrations or amounts reported for such peaks are most likely overestimated.
A 'Q' flag is used to indicate the presence of QC ion instabilities caused by quantitative
interferences. Affected analytes may be overestimated or underestimated as a result of this
interference. A peak is flagged 'Q' only if it is affected by a QC ion deviation greater than
20% full scale as determined relative to the labeled standard against which it is
quantitated. Total PCDF/PCDF quantitations will be flagged 'Q' if the interferences affect
ten percent or more of the total PCDD/PCDF peak areas.
An 'RO' flag is used to indicate that a labeled standard has an ion abundance ratio that is
outside of the acceptable QC limits, most likely due to a coeluting interference. This may
have caused the percent recovery of the standard to be overestimated. All quantitations
versus this standard, therefore, may be underestimated.
A 'U' flag is used to indicate that a specific (2,3,7,8-substituted) isomer cannot be
resolved from a large, coeluting interferent GC peak. The specific isomer is reported as
not detected as a valid concentration/amount cannot be determined. The calculated
detection limit, therefore, should be considered an underestimated value.
A *V flag is used to indicate that, although the percent recovery of a labeled standard may
be below a specific QC limit, the signal-to-noise ratio of the peak is greater than ten-to-
one. The standard is considered reliably quantifiable. All quantitations derived from the
standard are considered valid as well.
-------
Triangle Laboratories, Inc. September 11,1997
Case Narrative 43057r1
By our interpretation, the analytical data in this project are valid based on the guidelines
of EPA Method 23 (6/93) and Triangle Laboratories' Method 23 Data User's Manual.
Any specific QC concerns or problems have been discussed in the QC Remarks section of
this case narrative with emphasis on their effect on the data. Should Pacific
Environmental Services have any questions or comments regarding this data package,
please feel free to contact our Project Scientist, Amy Boehm, at 919/544-5729 ext. 268.
For Triangle Laboratories, Inc.,
Released by Final Quality Control Chemist
"Ah £..£..,
Sheila A. Lee-Lewis
Report Preparation Chemist
The total number of pages in the data package is : (6 7
-------
.T.yr?-
-V -, ; 3 pi •
TRIANGLE LABORATORIES, INC.
LIST OF CERTIFICATIONS AND ACCREDITATIONS
ENVIRONMENTAL
i" -
American Association for Laboratory Accreditation. Expires July 31, 1997. Certificate
Number 0226-01. Accreditation for technical competence in Environmental Testing.(lncluding
Waste Water, Sol/Haz Waste, Pulp/Paper, and Air Matrices) Parameters are AOX/TOX,
Volatiles, Pesticides, PCB's, BNA's, and Dioxin/Furan. Method 1613 for Drinking Water.
State of Alabama, Department of Environmental Management. Expires December 31,
1997. Laboratory I.D. # 40950. Dioxin in drinking water.
State of Alaska, Department of Environmental Conservation. Expires December 21,1997.
Certificate number OS-00397. Dioxin in drinking water.
State of Arizona, Department of Health Services. Expires May 26, 1998. Certificate
#AZ0423. Drinking Water for Dioxin, Dioxin in WW and S/H Waste.
State of Arkansas, Department of Pollution Control and Ecology. Expires February 18,
1998. Pulp/paper, soil, water, and Hazardous Waste for Dioxin/Furan; AOX/TQX.
State of California, Department of Health Services. Expires August 31, 1997. Certificate
#1922. Selected Metals in Waste Water; Volatiles, Semi-volatiles, and Dioxin/furan in WW and
Sol/Haz Waste. Dioxin in drinking water.
State of Connecticut, Department of Health Services. Expires September 30, 1997.
Registration # PH-0117. Dioxin in drinking water.
Delaware Health and Social Services. Expires December 31, 1997. Certificate #NC 140.
Dioxin in drinking water.
Rorida Department of Health and Rehabilitative Services. Expires June 30,1997.Dioxin in
DW. Drinking Water ID HRS# 87424. Metals, Extractable Organics (GC/MS), Pesticides/PCB's
(GC) and Volatiles (GC/MS) in Environmental Samples. Environmental water ID HRS#
E87411.
Triangle Laboratories, Inc.
Pn*.d«6fli7 801 Capitola Drive P.O. Box 13485
Durham, NC 27713-4411 Research Triangle Park, NC 27709-3485
919-544-5729 Fax * 919-544-5491 c
b
-------
Hawaii Department of Health. Expires March 1, 1998. Dioxin in drinking water. "Accepted"
status for regulatory purposes .
Idaho Department of Health and Welfare. Expires November 30, 1997. Dioxin in drinking
water.
State of Kansas, Department of Health and Environment. Expires January 31, 1998.
Environmental Analyses/Non potable Water and Solid and Hazardous Waste. Method 1613
for drinking water. ID #'s - Drinking water and/or pollution control - E-215. Solid or Hazardous
Waste -E-1209.
Commonwealth of Kentucky, Department for Environmental Protection. Expires
December 31, 1997. ID#90060. Dioxin in drinking water.
Maryland Department of Health and Mental Hygiene. Expires September 30, 1997.
Certification #235. Drinking water by Method 1613A.
State of Michigan, Department of Public Health. Expires March 31,1997. Drinking water by
Method 1613.
Mississippi State Department of Health. No expiration date.. Dioxin in drinking water.
Montana Department of Health and Environmental Services. Expires December 31, 1997.
Dioxin in drinking water.
State of New Jersey, Department of Environmental Protection and Energy. Extended by
state. Temporary certificate until June 30, 1997 or sooner. ID #67851. BNAs and Volatiles.
Dioxin in drinking water.
State of New Mexico, Environment Department. Expires July 31, 1997. Dioxin in drinking
water.
New York State Department of Health. Expires June 30, 1997. ID #11026. Environmental
Analyses of non-potable Water, Solid and Hazardous Waste. Method 1613 in DW.
State of North Carolina, Department of Environment Health and Natural Resources
Expires December 31, 1997. Certificate # 37751. Dioxin in drinking water.
State of North Carolina, Department of Environment, Health, and Natural Resources,
Division of Environmental Management. Expires December 31, 1997. Certificate # 485.
Metals, pesticides & PCBs, semi-volatiles and volatiles; TCLP.
North Dakota State Department of Health and Consolidated Laboratories. Expires
December 31,1997. Certificate # R-076. Effective October 4,1993. Dioxin in drinking water.
Rtvnwl 6/2W7 ,m
Pnrrtad 6/26/97
-------
Oklahoma Department of Environmental Quality. Expires October 31, 1997. Laboratory
#9612. Dioxin by 1613A, 8290 and 8280.
State of South Carolina, Department of Health and Environmental Control. Expires June
30.1997. Certificate number #99040001 (drinking water). Expires August 31, 1997. Certificate
number #99040002 (other parameters). Dioxin/Furans. BNA, Volatiles, and PCBs/pesticides
under Clean Water Act. 2.3,7,8-TCDD for Drinking Water, and Organic extractables for Solid
and Hazardous Waste.
State of Tennessee. Department of Environment and Conservation. Expires February 5,
1999. ID #02992. Method 1613 Drinking water only.
U.S. Department of Agriculture Soil Permit. Expires September 30, 2002. Permit No. S-
4958. Under the authority of the Federal Plant Pest Act, permission is granted to receive
foreign soil samples for use in laboratory analysis.
U.S. Army Corps of Engineers. Expires November 30, 1997. Validated; to perform methods
8280 & 8290 for Lockboume Landfill Site Investigation, Defense Distribution Depot Projects,
and assorted projects for the USAGE North PacifieDMsfon Laboratory.
U.S. EPA Region V. Expires November 14,1999. Dioxin in drinking water.
U.S. EPA Region VIII, for the State of Wyoming. Expires November 13, 1997. Dioxin in
drinking water.
State of Utah, Department of Health. Expires December 31, 1997. Certificate Number E-
166. Certification for the following parameters: Semi-Volatiies and Volatiles under RCRA;
Volatiles under Clean Water Act; Dioxin/furans by Method 8280; Drinking water for Dioxin by
Method 1613; Metals including Mercury and Microwave Digestion.
Commonwealth of Virginia, Department of General Services, Division of Consolidated
Laboratory Services. Expires June 30, 1998. ID # 00341. Dioxin in drinking water.
State of Washington, Department of Ecology. Expires September 11, 1997. Lab
Accreditation Number C067. Scope of Accreditation applies to water analyses for
Polychlorinated Dibenzo-p-dioxins and Polychlorinated Dibenzofurans, BNA Extr (Semivolatile)
Organics and Purgeable (Volatile) Organics.
State of Washington, Department of Health. Expires April 30,1998. Dioxin in drinking water.
Labl.D. 129
State of West Virginia, Department of Health. Expires December 31, 1997. Certificate No.
9923(C). Dioxin in drinking water.
Rmmd 676/97 jm
prwMd tnem
8
-------
State of Wisconsin, Department of Natural Resources. Expires June 30, 1997. Laboratory
ID Number 999869530. Certification for the following categories of Organics: Purgeable,
Base/Neutral, Acid, PCBs, and Dioxin. Expires November 14, 1999. Laboratory ID
999869530. Dioxin in drinking water.
PHARMACEUTICAL
Drug Enforcement Agency (DEA). Expires November 30. 1997. Registration number
RT01 195835. Controlled substance registration for schedules 1,2.3,3N,4,5.
N.C. Department of Human Resources. Expires October 31, 1997. Registration number
NC-PT 0000 0031 . North Carolina controlled substances registration. Application submitted for
renewal.
Food & Drug Administration (FDA) Registration. Expires July 1997. ID #'s 001500 1053481.
Annual registration of drug establishment. Annual registration of drug establishment.
OTHER
Clinical Laboratory Improvement Amendments (CLIA) Registration. Expires May 30, 1999.
ID # 34D0705123. Department of Health & Human Services, Health Care Rnancing
Administration.
U.S. EPA Large Quantity Hazardous Waste Generator. No expiration date. EPA ID
#NCD9821 56879. Permit indicates that the laboratory is a large generator of hazardous
North Carolina Radioactive Materials License. Expires April 30 1998. License No. 032-
0954-1 . License authorizes the licensee to receive, acquire, own, possess, transfer, import and
use such radioactive materials as designated.
North Carolina General License for Radiation Protection. No. expiration date. License No.
032-875-OG. The general license applies only to radioactive material contained in devices
which have been manufactured and labeled in accordance with specific requirements.
Printed 6T26/B7
9
-------
'.'-='
lAl'iLr.
DOCUMENT
CONTROL
Triangle Laboratories, Inc.
801 Capitola Drive P.O. Box 13485
Durham, NC 277134411 Research Triangle Park, NC 27709-348i
919-544-5729 Fax * 919-544-5491
-------
CHAIN OF CUSTODY
Sampler's Signature:
Company: PES. Inc.
Address: 5001 S. Miami
Blvd.
RTP. NC 27709-2077
Phone*: 919-941-0333
Location Sampled:
Inlet
inlet
Inlet
Inlet
Outlet
Outlet
Outlet
Outlet
Outlet
Outlet
Date:
8//1
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RecelvecHor Laboratory B
Time:
T-i$
•
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IMC
I
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8:3.2-
l-
Contact:
Project Name:
Project Location:
P.O. #:
Fax*:
Grab or Comp.:
Composite •
Composite
Composite .
Composite . *
Composite *
Composite *
Composite * •
Composite *
Composite
Composite •
Date/Time:
Dat
>/Tlnie: ^
y/Slgnature:
^^^
Mike Maret
A&W*fT*A*ir **"
Qarner, NC
919-941-0234
Field Sample I.D.#:
I-M23-1-XAD
i.
I-M23-1 -Ace/Toluene
I-M23-1 -Filter
I-M23-1-IMP
0-M23-1-XAD
O-M23-1 -Ace/Toluene
O-M23-1 -Filter
O-M23-1-IMP
O-M23-2-XAD
O-M23-2-Ace/Toluene
Received By:
Received By:
Date/Time:
"V"
Comment*:
* ot Cont.
/ /
1^
1 '
\ '
( s
\ '
1 /
( s
1 '
I '
Analysis Required:
Poty-chlorlnaled Oloxln/Furans
Poly-chlorinated Dloxln/Furans
Poly-chlorlnatad Dloxln/Furans
Poty-chlorlnated Dloxln/Furans
Poly-chlorinated Dloxln/Furans
Poly-chlorinated Dloxln/Furans
Poty-chlorlnated Dloxln/Furans
Poty-chlorlnated Dloxln/Furans
Poly-chlorinated Dloxln/Furans
Poly-chlorinated Dloxln/Furans
Relinquished By:
Relinquished By:
Send Samples To:
Date/Time:
Date/Time:
Remarks:
XAD
Ace/Toluene
Filler
ARCHIVE
XAD
Ace/Toluene
Filter
ARCHIVE
XAD
Ace/Toluene
Received By:
Received By:
Triangle Laboratories Inc.
801 Capltola Drive
Durham, North Carolina 27713
-------
1
, Company: PES. Inc.
r
CHAIN OF CUSTODY Sampler's Signature:
N --•
Address: 5001 S. Miami Blvd.
RTF, NC 27709-2077
H
i
' Phone*: 919-941-0333
> Location Sampled:
! Outlet
i
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Outlet
Outlet
Outlet
Cutlet
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Date:
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Time:
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Contact:
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Project Location:
P.O. #:
Fax#:
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Composite *
Composite *
Composite *•
Composite
Composite
Composite
Date/Tlme:
Date/Dme:
3y/Slgnature:
— ^— «^-^^
Mike Maret
ft A '*
ifsprttcr "PLftKfT A
Garner, NC
919-941-0234
Reid Sample I.D.#:
O-M23-2-FIHer
W-M23-2-IMP
0-M23-3-XAD
O-M23-3-Ace/Tduene
O-M23-3-Flller
O-M23-3-IMP
0-M23-FB-XAD
O-M23-FB-Ace/Tduens
O-M23-FB-Flller
O-M23-FB-IMP
Received By:
Received By:
DateATlme:
^ l~2.<~(fy~~~) /Z'
-------
r^(Q)
B) Yr ' ' «H
CHAIN OF CUSTODY Sampler's Signature:
Company: PES. Inc.
Address: 5001 S. Miami Blvd.
*
RTF. NC 27709-2077
Phone #:
Location Sampled:
Outlet — tOQ
Outlet
Outlet
Outlet
Outlet
919-941-0333
Date:
0-M-fr
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Relinquished By:
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Project Locution:
P.O. #:
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•
Date/Time:
Date/Time/ ,
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Received for Laboratory By/Signature:
/TS *S? S~* ~7 '
£
Field Sample I.D.#:
O-MtMilJOL.
0-M23-4-XAD
O-M23-4-Ace/Toluene
0-M23-4-Fllter
0-M23-4-IMP
•
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Received By:
Date/Time:
4 fa fit 17:^
Comments:
# of Cont
( '
\'
\ -
1 '
t« Treee Metal* Plut Ha
Poly-ohlorlnated Dloxln/Furani
Poly-chlorlnattd Dloxln/Furans
Poly-chlorlnaled Dloxln/Furant
Poly-chlorinated Dloxln/Furans
-
Relinquished By: Date/Time:
Relinquished By: Date/Time:
HCi
XAD
Ace/Toluene
Filter
ARCHIVE
Received By:
Received By:
Send Samples To: Tr/ang/e Laboratories, Inc.
,801 Capltola Drive
Durham, North Carolina 27713
-------
CHAIN OF CUSTODY Sampler's Signature:
Company: PES, Inc.
Address: 5001 S. Miami Blvd.
RTP. NC 27709-2077
Phone*: 919-941-0333
Location Sampled:
Date:
Relinquished By:
f^^O^L
Time:
,
Contact:
Project Name:
Project Location:
P.O. #\
Grab or Comp.:
Composite '*
Composite
Composite . *
Composite
Data/Time:
Datefllme:/ .^
Receive9T5rLaboratory By/Signature:
/ s jf x^° '^s' /^-^
Mike Maret
AsPHAtrTLfatr "A"
Gamer, NC
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919-941-0234
Field Sample I.D.#:
0-M23-RB-XAD
O-M23-RB-Ac»/Tolu«n« . ^
O-Ma3-RB-Fllter
0-M23-RB-IMP
•
Received By:
Received By:
Date/Time:
Comments:
# of Cont.
/ /
1 /
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Analysis Required:
Poly-chloflnaled Dloxln/Furant
Poly
-------
-TRIANGLE LABORATORIES, INC. -- UXJ IN RECORD/CHAIN OP CUSTODY*
Custody Seal Abnent Sample Seals i Absent
Chain of Custody Present Container. , . t Intact
Sample Tags Absent
Sample Tag Numbers Not Listed on Chain of Custody
SMO Forms N/A ' -
TLI Project Number 43057 , Book |
Client i PSC01 - PES, Inc. ' I
181 T
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.teReoe^ved JO./2V" | ^^^^^L **•
Ice Cheat/Box ICE Temp 19.0 C j Carrier and Number | PRANK PHOENIX ' 27
|TLI Number Client Sample ID Matrix
jjmR/HiCPM. Client COC ID * Location
|m-27-lA I-M23-1-XAD XAD
| I-M23-1-XAD C02
1-
—
(181-27-1B I-M23-1-ACE/TOLUBNB ACE/TOLUENE
1 I-M23-1-ACB/TOLUBNB C02
|181-27-lC I -M23-1 -FILTER FILTER
| I-M23-1-FILTER C02
|l81-27-!D I-M23-1-IMP IMP
| I-M23-1-IMP C02
|l81-27-2A 0-M23-1-XAD XAD
| O-M23-1-XAD ' C02
|l81-27-2B 0-M23-1-ACB/TOLUENB ACE/TOLUENE
jj 0-M23-1-ACB/TOLUENB C02
|l81-27-2C O-M23-1-PILTER FILTER
| 0-M23-1-FILTER C02
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|iei-27-2D 0-M23-1-IMP ' . IMP
| O-M23-1-IMP C02' .
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|l81-27-3A O-M23-2-XAD XAD
| O-M23-2-XAD C02
•
|l81-27-3B 0-M23-2-ACE/TOLUEHB ACE/TOLOBHB
| 0-M23-2-ACB/TOLUENE C02
— "
(181-27-3C 0-M23-2-FILTER FILTER
| 0-M23-2-FILTER • . C02
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|l81-27-3D 0-M23-2-IMP IMP
| 0-M23-2-IMP C02
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|l81-27-3E 0-M23-2-IMP IMP
| O-M23-2-IMP C02
|!81-27-4A O-M23-3-XAD XAD
| 0-M23-3-XAD C02
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Date/Init
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1 Receiving Remarks: SAMPLES DELIVERED IN 3 BOXES AND 1 COOLER. ICB IN COOLER HAS HATER WHEN RECIEVED.
| 0-M2I-RB-XAD HAS NOT WITH SHIPMENT.
I Archive Remarks i
To LAB
Date/Init
To STORAGE | DISPOSED
Date/Inlt Date/Inlt
• .
1
1
SAMPLE
•
-------
Custody Seal t Absent Sample Seals t Absent
Chain of Custody t Present Container...! Intact
Sample Tags t Absent
Sample Tag Numbers > Hot Listed on Chain of Custody
SMO Forms i H/A '-
TLI Project Number 43057 , Book |CD
Client i PSCOl - PES, Inc. ' |e»H
„ f "I
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Date Received j 08/29/97 j "S^^'^^^^'a'
Ice Chest/Box ICB Temp 19.0 C Carrier and Number | FRANK PHOENIX ' 27
|TLI Number . . . Client Sample ID .Matrix
jjmR/HiCPM . Client COC ID .. • location
».
|!81-27-4B 0-M23-3-ACE/TOUJENE ACE/TOLUENE
| 0-M23- 3 -ACE/TOLUENE C02
. .. .. _., ,
|lBl-27-4C O-M23-3-FILTBR FILTER
| 0-M23-3-FILTBR C02
_. ... . . .
|l81-27-4D 0-M23-3-IMP IMP
| O-M23-3-IMP C02
------
|l81-27-4B 0-M23-3-IMP IMP
| O-M23-3-IMP C02
• - -
|l81-27-SA 0-M23-FB-XAD XAD
| O-M23-FB-XAD CO 2
|l81-27-5B 0-M23-FB-ACE/TOLUBNE ACB/TOURNB
| O-M23-FB-ACE/TOLUENB C02
" ' '
(181-27-SC 0-M23-FB-FILTER FILTER
| 0-M23-FB-FILTER C02
—
(181-27-5D 0-M23-FB-IMP '. IMP
| 0-M23-FB-IMP C02'.
To LAB
Date/Init
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| O-M23-4-XAD C02
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| 0-M23-4-ACB/TOUJENE C02 "«JfV
|!81-27-6C 0-M23 -4 -FILTER FILTER
| 0-M23-4-FILTBR •>. C02
|l81-27-6D 0-M23-4-IMP IMP
| 0-N23-4-IMP CQ2
|!81-27-7A O-M23-RB-ACB/TOLUENB ACB/TOLUEHB
| 0-M23-RB-ACE/TOLWENB C02
.
|!81-27-7B O-M23-RB-FILTBR FILTER
| O-M23-RB-FILTER C02
t
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Date/Init
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1 Receiving Remarks t SAMPLES DELIVERED IN 3 BOXES AND 1 COOLER. ICB IH COOLER HAS HATER HHEN RECIBVBD. 8AMPLB
| 0-M23-RB-XAD HAS NOT NITH SHIPMENT.
1
1 Archive Remarks!
-------
Custody Seal t Absent Sample Seals t Absent
Chain of Custody i Absent Container...! Intact
Sample Tags : Absent
Sample Tag Numbers i Not Listed on Chain of Custody
SMO Forms t Absent
TLI Project Number 43113 , Booktj"
Client: PES03 - Pacific Environmental Services ff>
181
Date Received \ 09/05/97 \ By S/'ffllstSj^i s**T**$*
- •" ~ ~ 1 • ••ycr 'f i
NO COOLANT Carrier and Number 1 DEBBIE HAQB ' 1 83
m i'
|mR/HiCPM. Client COC ID * Location
1
|m-83-l Reagent Blank Xad XAD
1 no C.O.C. * C01
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*
'
To LAB To STORAGE
.Date/Init Date/Inlt
LAl. ">rJ
?/£/f7 /M
'
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Date/Inlt Date/Inlt Date/Inlt Date/Inlt
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-
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| 1
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.
DISPOSED
Date/Init
Receiving Remarks i Debbie Hage said this was a sample Chat Belonged to client. ,
No paperwork arrived with samples i CLIENT needs to provide a Chain of Custody with sample IDs
matching the sample labels.
Archive Remarks i
•Form Revised 05/27/1997 — Page 1 OF 1-
-------
TRIANGLE LABORATORIES, INC.
SAMPLE TRACKING AND PROJECT MANAGEMENT FORM
ADMINISTRATIVE INFORMATION
TLI Proj#: 43057-rl Samples: 1 TurnAround.: 7 Day(s)
Prod Code: D23061 Matrix.: M23Train Hold Time..: 30 Day(s)
DetectLim: 0.05 ng Type...: A Start Date.: 09/05/97
Recvd. . : 08/29/97 Ship By : 09/11/97 ^
DWL Due Dt.: 03/OD/D7—
Analyte List.: tetra-octa PCDDs/PCDFs
Method : Method 23 :Tetra-Octa (Tol Combined)
Client Proj . . : ASPECT T>Liv*r "A"
Client : Pacific Environmental Services (PES03)
P.O. No : 104-98-0019 & -0020 Collect Dt/Tm: SeeCOC
Contact : Mike Maret Phone : 919-941-0333
Proj. Mgr : Amy J. Boehm Fax : 919-941-0234
Sample Origin: NC
SPECIAL INSTRUCTIONS / QA REQUIREMENTS
Prep Project: 03804 Prespike Standard: USF-CS
Prespike Amount..: 4.Ong
Extraction Exp...: 09/18/97
-------------------------- REPORTING REQUIREMENTS
Reporting Format: Report Option II
See MILES for Instructions/Communications.
by: ^TE:
Reviewed by: d DM, (PMGT0197)
Triangle Laboratories, Inc.® Analytical Services Division
801 Caprtola Drive • Durham, North Carolina 27713 Printed: 11:07
Phone: (919) 544-5729 • Fax: (919) 544-5491 jfe,.
-------
PROJECT COMMUNICATION TRACKING FORM
TL1 Project Number:
b / 1:
Use this form to record all exchanges of information between production units as well as personnel
handling -this project. Decisions, corrective actions and recommendations must also appear on this
tracking document
Name
Comment / Decision / Resolution / Action / Observation
PSC01-PES, Inc.
I-M23-1-FILTER
Rr-oject : 4-3O57
1 S1-27-1C
PSC01-PES, Inc.
I-M23-1-XAD
Rr-ojeo-t: 4-3O5 7
1 © 1 —27—1 A
I hlW • voV>»-fe
M
PSC01-PES, Inc.
0-M23-1-FILTER
ct :-4-3O57
—27—2O
-
••
•
PSC01-PES, Inc.
0-M23-1-XAD , (
Rr-oJ eot : 4-3057 4 <*3 VMe^l
1 e 1 -27— 2A . J
:••.-• ' \
PSC01-PES, Inc. "• . J
0-M2y-^-HlLlbH v/A-^ » - »
Rr-odect : 4-3057 '.Xft^>-^'^^T^ ' «
iei-27 — 3C -'. Xl1 •»•//
\C'A^^ u^v^,-fe /b/QvJv^
PSC01-PES, Inc. I r ^ /
O-M23-2-XAD
Rr-oJ oot : 4-3057 r . ..,,11
^ 0 -. ~^ ^A ' ^rr<&' ^^P\)
181 — ei I +3 r\ j- L s
'Jf
•
•
19
-------
i r u/-u »%••— — --- .....
PROJECT COMMUNICATION TRACKIN'G FORM
page j2_ of
TL1 Project Number:
Use this form to record all exchanges of information between production units as well as personnel
handling -this project. Decisions, corrective actions and recommendations must also appear on this
tracking document
ate
Name
Comment / Decision / Resolution / Action / Observation
PSC01-PES, inc.
0-M23-3-XAD
sct : 4-3057
XfVD -
PSC01-PES, Inc. '
0-M23-3-FILTER-
ject : 4-3057
1 61 — 27— 4-C
PSC01-PES, Inc.
0-M23-FB-XAO
o j & o -t : -4- 3 O S 7
1 ©1 —27— ,5 A
PSC01-PES, Inc.
0-M23-FB-FILTER
1 S 1 — 27 — 5C
PSC01-PES, Inc.
O-M23-4-XAO
ct: -4-3O57
— 27— eA
PSC01-PES, Inc.
0-M23-4-FILTER
oot : -4-3057
1 — 27 — ©o
/Hlf,
if.
PES03-Pac1f1c Environmental Services
Reagent Blank Xad
Pr-ojeotr^-SI 1 3
1S1—©3—1
PSC01-PES, Inc.
0-M23-RB-FILTER
F*»-oJoot : 4-3057
1 © 1 —27 — 7B
20
-------
ject: 43057
sent (s) /Acid (3) :
Numbers :
Spike: Ml
Spike: 0 Ml
Spike: 0 M!
Spike: _20 Ml
| TLI /
rd| SAMPLE /
I ID /
| TLI Blank
1
| 181-27-AA-C
1
| 181-27-2A-C
1
| 181-27-3A-C
1
| 181-27-4A-C
1
| 181-27-SA-C
1
| 181-27-6A-C
1
| 181-27-7AB4
| TLI LCS
1
| TLI LCSD
1
TRIANGLE LABORATORIES, INC.
Dioxin Sample Preparation Tracking t Management Fora
Client: Pacific Em
"f^lll&^L^ / 1 Method: Method 23:Tetra-Oeta
^f'/Sfif 1 1 Extraction Date: V / b l~7/
cone: . nq/Ml 1 _~:£l_™, ' ^-M '
cone: 0.0000 nq/fil | J *• JT JL \jZ*JVj 1
cone: 0.0000 ng/Ml 1 1/5 fcjX 1 US )~ fW 1
cone : _0 . 01 ng/Ml 1 .i. 1 ji Ijae 1 13? 1 LZ /jt/1
| GROSS | SAMPLE | /*/ : QQ \ /*/ : 7^3 |
CLIENT | WEIGHT | SIZE | 0-f nq/ltl | O.Qf nq/Ml |
SAMPLE ID | Before After 1 ej / nl 1 ^£) ul 1 YD ul 1
1 1 1 1 % /? 1 1
TLI M23 Blank | -— f " | J I £*C . O . | |
1 1 1 1 / s? 1 1
I-M23-1 | — ~| | ItXl ' (~- ' \ ' 1
1 ' \^ \ \ ., /> 1 1
0-M23-1 | — -T _ 1 I 1 ^C. • C . 1 1
1 K, 1 1 / - 1 1
0-M23-2 | -*\ \ \&t-' (^ , 1 1
0-M23-3.,| *| | !£<-•< O- 1 1
1 1^ 1 1 .- 1 1
0-M23-FB | "^*| | | /£_ . (_,. I 1
'1 1 1 1 / /} 1 1
0-M23-4 | -"-r"~ | 1 &C . C-, 1 1
1 1 1 ' / X? ' /• '
TLI LCS i — r~ i 1 i tX— . o< ~L0*-' *—• i
TLI LCSD | | | |£^~ ' (-*'* JkX-1 .1
rironmental Ser
(Tol Combined)
^9tf i
*li^ Bl
_3 / 08/^^1
0-1 na/ul |
WO Ml 1
ms !
ms !
pos !
ms !
WS !
Ms !
ms !
ms !
iris i
MS \
PAGE 1 OF 1
vices (PES03)
Matrix: XXK>
AV/S
-------
PAGE 1 OF 1
IK1AMUUS IjABUKAlUKXCS , INC .
DIOXIN SAMPLE EXTRACTION and CLEANUP TRACKING FORM
TLI Project No.: 430S7
Ext Stt.crd and | °| | | | |
TLI Number | |. | £ 1 ^ 1 4? 1 3 1
ooo | ./. lA^^l 1 I>^V\I>
TLI Blank \ /-•//> 7 *y\Y\5 ' WlC ' ^^ ' ft/w '*
181-27-1A-C |
. ....
002 |
181-27-2A-C |
003 |
181-27-3A-C |
004 |
181-27-4A-C |
005 |
181-27-5A-C |
006 |
181-27- 6A-C |
007 |
181-27-7AB& |
008 |
TLI LCS |
009 | '^
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1 1
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Enter the procedure number below into the box at the top of each column to signify the step performed.
Initial and date each sample for each numbered procedure performed.
i_ PROCEDURE DETAILS (circle)
-
ON_f^OFF (fgxSiieFy Jar / Sep Funnel / Steam Dist / Cont LL / ASS / Waste Dilution
)SPIKE AFTER EXTRACTION ^
>ADD TRIDECANE
40mL / <32mV /
5) COMBINE
^&P DIVIDE / LXPID DETERMINATION 2Q*/80* (%0\/SO&* 5«L/20mL Other
'SOLVENT EX _^
CLEANOP/ ^^/r/tC^^^m^' DSP 26Q? / DSP 225 / DSP 115 / DSP 215 / DSP 267 / Other
iTRANSFER
10) ADDITIONAL CLEANUP
11) FINAL TRANSFER
Mod. DSP 260 / DSP 225 / DSP 115 / DSP 215 / DSP 267 / Other
Comments:
......Rev 06/24/97 (PSTMP 4).
Jfc
22
-------
PAGE 1 OP 1
TRIANGLE LABORATORIES. INC.
DIOXIN SAMPLE EXTRACTION and CLEANUP TRACKING FORM
TLI Project No.: 43057 rl
. Stt.crd and
! I
. Number | ^ |
-------
PAGE 1 OF 1
TRIANGLE LABORATORIES, INC.
Transfer Chain-of-Custody Form
Project 43057-rl
Transfer From: DWLH5 To: DMS5
Initials.. Date
Released by:
Accepted by.
Time...
MILES.ID.
TLI No Gust. Id.
43057-rl -000
43057-rl -006
TLI Blank
181-27-6A-C
TLI M23 Blank
O-M23-4
Additional comments or instructions:
-XfrCOC (Rev 11/01/94)--+
24
-------
PAGE 1 OF 1
Method: Method 23:Tetra-Octa (Tol
Required Detection Limit: 0.05 ng
I TLI /
crd| SAMPLE ID / CLIENT
| / SAMPLE ID
| TLI Blank
| 181-27-6A-C
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
Zommenta :
TRIANGLE LABORATORIES, INC. I
| PROJECT: 43057rl |
SAMPLE INFORMATION RS Cone I
1ST COLUMN 2ND COLUMN 20 /il 9 100.0 PG//U |
| GC/MS FILENAME (CONFIRM [CONFIRM FILENAME (DSF-RS |OSF-RS (ANALYSIS 1
1 COLUMN: r7i4^ 1 1 COLUMN : ^f^W)"" 1 VOLUME f*J| I INIT. f*** 1 COMMENTS 1
| | | |S<2LN ID (DATE ^_| |
1 II III 1
1 II 1 1 1 1 1 1
i ^SQ,£ i -\ ' ^i i c/ ivy i '
i i ' i iii i
i ii iii i
i ii iii i
i ii iii i
i ii iii i
i ii iii i
i ii iii. i
i ii iii i
i ii iii i
i ii iii i
i it fit i
i ii iii i
i ii iii i
i ii iii i
i ii iii i
i ii iii {
i ii iii i
i ii iii t
i ii iii i
i ii iii i
i
Type: A 1
1
1
1
SDike File: SPXZ3704 |
1
Amc of Extract: 50% |
PEV m/m./<>s (psiMp ci — *.
25
-------
lilMiiglol nnoiMiniltifl, Ilic
HUM Log
CT5
Instrument ID Column Tvoe Column ID plot Name Inj. Vol. Acquisilion G/C_
-70-5 n :
99
-------
Triangle Laboratories, Inc.
Run Log
Instrument ID
Column Type
on
Column ID
Plot Name
Tt-1
Acquisition
Signature
G/C
Date
Filename
Date*
Time*
Project*
Sample*
No.
Client Sample ID
Syr
332
Operator/Dale
Comments*
G L
,
PC
fa-C
181 -
V
-fcXV
t-t
0
£
V
9 l
,
i\4l
i
Ml
* Transcribed from chromatographic data
** Dated initials required
stvr1/qa/forms/hrrunlog.doc (02/05/97)
ConCal Due:
ConCal Due:
-------
SAMPLE
DATA
Triangle Laboratories, Inc.
801 Capitota Drive P.O.Box 13485
Durham, NC 277134411 Research Triangle Park, NC 27709-341
919-544-5729 Faxi 919-544-5491
Ik.
28
-------
TRIANGLE LABORATORIES, INC. Page 1
Sample Result Summary for Project 43057rl 09/14/97
Method 23X Full Screen Analyses (DB-5)
Data File S975864 S975865
Sample ID TLI M23 Blank 0-M23-4
Units ng ng
Extraction Date 09/06/97 09/06/97
Analysis Date 09/13/97 09/13/97
Instrument S S
Matrix XAD M23TRAIN
Extraction Type
Analytes
2378-TCDD (0.004) (0.004)
12378-PeCDD (0.005) (0.005)
123478-HxCDD (0.006) (0.006)
123678-HxCDD (0.005) 0.01
123789-HxCDD (0.005) (0.005)
1234678-HpCDD 0.03 {0.04} B
OCDD 0.04 0.09 B
2378-TCDF 0.008 0.02 B
12378-PeCDF (0.004) (0.003)
23478-PeCDF {0.007} {0.01} B
123478-HxCDF 0.03 0.03 B
123678-HxCDF 0.01 0.01 B
234678-HxCDF 0.02 0.02 B
123789-HxCDF (0.004) (0.004)
1234678-HpCDF 0.05 0.05 B
1234789-HpCDF 0.02 0.02 B
OCDF 0.03 0.05 B
TOTAL TCDD 0.009 {0.007}
TOTAL PeCDD {0.03} 0.01
TOTAL HxCDD 0.05 0.07
TOTAL HpCDD 0.06 {0.07}
TOTAL TCDF 0.008 0.03
TOTAL PeCDF {0.007} 0.01
TOTAL HxCDF 0.08 0.09
TOTAL HpCDF 0.08 0.09
Other Standards Percent Recovery Summary (% Rec)
37C1-TCDD 105 106
13C12-PeCDF 234 87.7 93.4
13C12-HxCDF 478 93.9 97.6
13C12-HxCDD 478 89.6 85.9
13C12-HpCDF 789 107 98.7
Other Standards Percent Recovery Summary (% Rec)
13C12-HxCDF 789 97.3 117
13C12-HxCDF 234 84.8 107
Internal Standards Percent Recovery Summary (% Rec)
13C12-2378-TCDF 92.5 120
13C12-2378-TCDD 80.9 98.7
13C12-PeCDF 123 92.4 107
13C12-PeCDD 123 100 112
Triangle Laboratories, Inc.® Analytical Services Division
801 Capitola Drive • Durham. North Carolina 27713 Printed-17-52 09/14/97
Phone: (919) 544-5729* Fax: (919) 544-5491 '
-------
TRIANGLE LABORATORIES. INC.
Sample Result Summary for Project 43057rl
Method 23X Full Screen Analyses (DB-5)
Page 2
09/14/97
Data File
S975864
Sample ID TLI M23 Blank
Units
Extraction Date
Analysis Dace
Instrument
Matrix
Extraction Type
Internal Standards
12C12-HxCDF 678
12C12-HxCDD 678
13C12-HpCDF 678
13C12-HpCDD 678
13C12-OCDD
ng
09/06/97
09/13/97
S
XAD
Percent Recovery
92.8
83.6
72.2
85.0
67.5
S975865
0-M23-4
ng
09/06/97
09/13/97
S
M2 3 TRAIN
Summary (%
113
103
88.5
90.1
68.8
Rec)
{Estimated Maximum Possible Concentration}, (Detection Limit)
Triangle Laboratories, Inc.® Analytical Services Division
801 Caprtola Drive • Durham. North Carolina 27713
Phone: (919) 544-5729 • Fax: (919) 544-5491
Printed:! 7:52 0&
-------
TRIANGLE LABORATORIES, INC. Page 1
Sample Result Summary for Project 43057rl 09/14/97
Method 23X (DB-225)
Data File P973848 P973849
Sample ID TLI M23 Blank O-M23-4
Units ng ng
Extraction Dace 09/06/97 09/06/97
Analysis Date 09/12/97 09/12/97
Instrument P P
Matrix XAD M23TRAIN
Extraction Type
Analytes
2378-TCDF (0.008) (0.01)
Internal Standards Percent Recovery Summary (% Rec)
13C12-2378-TCDF 72.7 104
(Detection Limit).
Triangle Laboratories, Inc.® Analytical Services Division
301 Caprtola Drive • Durham, North Carolina 27713 Printed: 17:56 W/14/97
3hone: (919) 544-5729 • Fax: (919) 544-5491 J *
-------
TLI Project: 43057rl
Client Sample: TLI M23 Blank
Method 23 PCDD/PCDF Analysis (a)
Analysis File: S975864
Client Project:
Sample Matrix:
TLI ID:
Sample Size:
Dry Weight:
GC Column:
AsPM'fc-T -r*-t*rr "A"
XAD
TLI Blank
1.000
n/a
DB-5
Date Received:
Date Extracted:
Date Analyzed:
Dilution Factor:
Blank File:
Analyst:
II
09/06/97
09/13/97
n/a
S975864
ML
Spike File:
ICal:
ConCal:
% Moisture:
% Lipid:
% Solids:
SPX23704
SF56117
S975861
n/a
n/a
n/a
A fafere ^'<*+S'
.Anaiytes
2,3,7,8-TCDD
12,3,7,8-PeCDD
U.3,4,7,8-HxCDD
1,2,3,6,7,8-HxCDD
U.3,7,8,9-HxCDD
1,2,3.4,6,7,8-HpCDD
12,3,4,6,7,8,9-OCDD
2,3,7,8-TCDF
1,2,3,7,8-PeCDF
2,3,4,7,8-PeCDF
1,2,3,4,7,8-HxCDF
12,3,6,7,8-HxCDF
2,3,4,6,7,8-HxCDF
U.3,7,8,9-HxCDF
1,2.3,4,6,7,8-HpCDF
U.3,4,7,8,9-HpCDF
U.3,4,6,7,8,9-OCDF
Totals * " , , ,
Total TCDD
Total PeCDD
Total HxCDD
Total HpCDD
Total TCDF
Total PeCDF
Total HxCDF
Total HpCDF
*s &.ft«t * tnt4\:> ^' -*ft* >>jttfe'*'^pt* vy
* #%MW» \«y/" 'T1 wt*. _£ ^
ND 0.004
ND 0.005
ND 0.006
ND 0.005
ND 0.005
0.03
0.04
0.008
ND 0.004
EMPC
0.03
0.01
0.02
ND 0.004
0.05
0.02
0.03
Atnt- (09) , ftonsbe^-: uL.
0.009 1
EMPC
0.05 2
0.06 2
0.008 1
EMPC
0.08 6
0.08 3
|||i«pgi'v^s ^? liflftb^"*"1*4*'-5^? s**%'*Ftftd*
^^W^**X v. ,'N * , % . . , , •> s ','••' "«»**
_^^
_^_
__ __^
1.08 32:45
053 35:18
0.78 2135
.T.
0.007
125 29:11
122 29:16
1.18 29:46 1L
.^^_
1.12 31:55
1.14 33:06
0.88 35:25
:x jaw? ; , , >;; ;>,; 4 V~^ ^ ^ ,&*s* •
o.o3 n
^^^
—
0.007
.-
0.10
Page Iof2
X237 JfSH vXOO. LARS 6.1004
Triangle Laboratories, Inc.®
801 Capitola Drive • Durham, North Carolina 27713
Phone: (919) 544-5729 • Fax: (919) 544-5491
Printed:! 7:42
-------
'LI Project: 43057rl
:iient Sample: TLI M23 Blank
Method 23 PCDD/PCDF Analysis (a)
Analysis File: S975864
infernal Standards
C,2-2,3,7,8-TCDF
C,2-2,3,7,8-TCDD
C,2-l,2,3,7,8-PeCDF
C,2-l,2,3,7,8-PeCDD
C,2-l,2,3,6,7,8-HxCDF
C.2-l,2,3,6,7,8-HxCDD
C,:-l,2,3,4,6,7,8-HpCDF
C,2-l,2,3,4,6,7,8-HpCDD
C,2-1,2,3,4,6,7,8,9-OCDD
Surrogate Standards (type A)
CL,-2,3,7,8-TCDD
C,2-2,3,4,7,8-PeCDF
C12-l,2,3,4,7,8-HxCDF
C12-l,2,3,4,7,8-HxCDD
C,2-l,2,3,4,7,8,9-HpCDF
(Mtemaie Standards (Type A) ..
C12-l,2,3,7,8,9-HxCDF
C,2-2,3,4,6,7,8-HxCDF
Recovery Standards
:,2-l,2,3,4-TCDD
C,2-l,2,3,7,8,9-HxCDD
Amt (ng) - % Recovery QC limits -
3.7
3.2
3.7
4.0
3.7
3.3
2.9
3.4
5.4
Awt, (tl£) *,".,K
4.2
3.5
3.8
3.6
4.3
ilafcC^V-V-^
3.9
3.4
'".. •.* - '^"-T'
92.5
80.9
92.4
100
92.8
83.6
72.2
85.0
67.5
* Recover
105
87.7
93.9
89.6
107
^Recover
97.3
84.8
•o ^ ;
40%-130%
40%- 130%
40%- 130%
40%-130%
40%-130%
40%-130%
25%-130%
25%-130%
25%-130%
r •. *2^^ *ivBMlCJ&'
"" ^T •. •;rT '<
70%-140%
70%-140%
70%-140%
70%-140%
70%-140%
^ OCE k|»^is
40%-130%
40%- 130%
% .. -. x •. i. v
*" " '^ % "" •" v ^S--$& * -.
%.-5- ^ v*
0.77
0.78
1.44
1.48
0.51
1.23
0.44
1.02
0.92
;&***
1.42
0.51
1.21
0.41
^f\ Rafli*-?
0.51
0.50
^'*&&'
0.81
1.22
;^frcv::Ffass^
21:35
22:20
25:40
26:44
29:16
29:58
31:54
32:44
35:17
*> , injjs- !&»a& \
22:22
26:23
29:10
29:53
33:05
,;;K;8T^r*kgs.
30:28
29:46
*^R%|\;:^«f^
22:09
30:15
Data Reviewer
Page 2 of 2
09/14/97
X237j>SR vioa LARS «.io.o*
•jangle Laboratories, Inc.*
)1 Capitola Drive • Durham, North Carolina 27713
none: (919) 544-5729 • Fax: (919) 544-5491
Printed: 17:42 09/14/9
-------
Initi
Data Review By:
....Date...
Calculated Noise Area:
2.04
The Total Area for each peak with an ion abundance ratio outside
ratio limits has been recalculated according to method requirements.
Page No. 1
09/14/97
Compound/
M_2.... QC.Log omit Why
Listing of S97S864B.dbf
Matched GC Peaks / Ratio
/ Ret. Tine
.RT. OK Ratio Total.Area... Ar»a.E«*k.1.. Area.Peak.2.. Rel.RT Compound.Name.. ID.. Flags.
TCDF
304-306
D
D
304-306
13C12-TCDF
316-318
DC
DC
DC
DC
DC
d
d
DC
DC
DC
DC
NL
SN
SN
SN
SN
SN
SN
SN
SN
1
NL
HL
0:00
19:
19:
20:
20:
20:
21:
21:
21:
23:
27
49
07
31
47
09
25
35
22
0.
RO
RO
RO
RO
RO
RO
RO
65-0.39
0
0
0
1
0
0
0
0
0
0
.31
.60
.64
.80
.63
.87
.71
.36
.78
.42
Peak
0:
20:
21:
00
31
09
0.
RO
21:35
316-318
TCDD
320-322
D
320-322
37C1-TCDD
328
DC
d
DC
DC
DC
DC
DC
DC
DC
DC
DC
DC
DC
DC
3
NL
SN
SN
SN
SN
SN
SN
SN
SN
SN
SN
SN
WH
WH
1
22:
03
RO
0
3
3
1
4
6
7
1
14
4
14
.37
.86
.70
.63
.25
.05
.79
.72
.82 6.50
.46
.82
65-0.89
0
0
0
0
1
Peaks
0:
19:
20:
20:
21:
22:
22:
00
41
05
36
23
09
14
22:23
22:
22:
22:
23:
23:
23:
23:
37
48
59
10
18
36
36
0.
RO
RO
RO
RO
RO
RO
RO
RO
RO
RO
.91
.65
.72
.77 5
.13
5
65-0.89
1
0
0
1
1
1
0
0
0
1
0
0
0
0
1
.13
.85
.83
.90
.78
.74
.88
.35
.92
.24
.82
.62
.70
.32
.54
Peak
1
.13
35.70
26
.889
19
.06 10.91
.86 2.569.27
,45 12.3*
0.338-1.092
0.
0.
0.
0.
0.
0.
0.
0.
8.32 1.
1.
000
901
918
932
951
963
980
992
000 2378-TCDF
083
0.954-1.046
0.
0.
000
951
15.15 0.980
3,320.59 1.
10.99 1.
000 13C12-^37B-TCEP
022
.935.37
0
10
8
0
1
1
3
2
1
0
2
0
2
0
0
10
.27
.98 5.06
.33
.69
.15
.49
.32
.67
.95
.60
.02
.71
.29
.46
.50
.98
0.875-1.055
0.
5.92 0.
0.
0.
0.
0.
0.
1.
1.
1.
1.
1.
1.
1.
1.
000
881
899
922
957
992
996
002 2378-TCDD
013
021
029
037
043
057
057
0.910-1.090
DC
NL
0:
20:
00
57
0
7
.43
.76 7.76
0.
000
0.938
AN
AN
Triangle Laboratories, Inc.® Analytical Services Division
801 Capitola Drive • Durham, North Carolina 27713
Phone: (919) 544-5729 • Fax: (919) 544-5491
Printed: 17:42 09/14^4
-------
"age :.: .
Listing of S975864B.db£
Matched GC Peaks / Ratio / Ret. Time
I_Z. . . QC.Log Omit Why ..RT. OK Ratio Total. Area... Area. Peak. 1. . Area. Peak. 2. . F.«l. RT Compound. Name.. ID.. Flags.
22:22
128 2 Peaks
.3Ci:-?CDD
132-33-1 DC NL 0:00
21:07
22:09
22:20
22:41
I32-3--1 4 Peaks
'eCDF
I40-2i2 DC NL 0:00
DC SN 23:39
DC SN 24:20
DC SN 24:40
D d SN 25:17
DC SN 25:41
DC SN 25:58
D d SN 26:13
M 26:23
DC SN 26:51
DC SN 27:21
DC WH 27:49
40-342 1 Peak
3C12-PeCDF
52-354 DC NL 0:00
24:47
25:17
25:40
25:49
25:57
26:13
26:23
27:20
52-354 8 Peaks
eCDD
56-353 DC NL 0:00
24:56
25:40
25:59
26:13
DC SN 26:46
DC SN 26:58
DC SN 27:12
DC SN 27:23
0.
RO
RO
RO
1.
RO
RO
RO
RO
RO
RO
RO
1.
RO
1.
RO
RO
RO
RO
RO
RO
RO
RO
65-0.89
3
1
0
0
0
32
0
0
1
0
1
1
0
1
1
1
0
0
.15
.00
.81
.78
.94
___ AKrt
-1.78
.59
.61
.47
.57
.66
.64
.49
.71
.12
.47
.70
.28
3,679
3,687
0
22
4,831
4,164
53
9,071
vvf i^Lfi
0
2
4
1
10
5
2
7
10
3
2
0
10
.73
.49
.73
.53
.26
.20
.79
.78
n /
LJ f
.33
.01
.70
.84
.94
.20
.70
.66
.28
.06
.88
.39
.28
3.6-9.73
12.71
2,158.80
1 . 825 . 02
28.64
6.25
0.91:-
12
2,672
2,339
30
.73
.46
.18
.39
; _
C .
; .
1 .
1 .
0.915-
5
32-1.78
0
1
1
1
1
1
1
1
1
32
1
1
1
1
3
0
1
0
1
.82
.61
.45
.44
.35
.43
.64
.42
.33
iXi-iu
-1.78
.10
.26
.15
.89
.65
.78
.10
.62
.35
0
61
27
5,059
16
29
27
4,305
17
9,544
0
7
8
7
8
2
0
1
1
.23
.90
.10
.33
.10
.14
.67
.66
.65
.55
V /
f /
.18
.77
.87
.91
.98
.98
.92
.15
.08
38.19
16.06
2,983.33
9.25
17.16
17.20
2,528.87
10.09
4.72
5.39
5.87
12.84
23
11
2,076
6
11
10
1,776
7
3
4
3
3
.60
0.
.71
.04
.00
.85
.98
.47
.79
.56
0.
.76
.68
.10
.52
C .
0.
A
G.
0.
1.
1 .
1 .
1.
1 .
1, .
i.
301 37C1-TCDD
1.090
300
946
992 13C12-1234-TCDD
300 13C12-2378-TCDD
316
1.074
300
921
948
961
985
001 12378-PeCDF
012
021
028 23478-P«CDF
046
066
084
SDR1
RSI
IS1
AN
AN
844-1.156
0.
0.
0.
1 .
1.
1 .
1.
1 .
1 .
000
966
985
000 13C12-PeCDF 123
006
Oil
021
028 13C12-PeCDF 234
065
IS2
SUR2
926-1.024
n f
Q.
0.
0.
0.
i .
^ .
1 .
i.
000
933
960
972
981
001 12378-PeCDD
309
017
324
AN
Jangle Laboratories, Inc.® Analytical Services Division
11 Caprtola Drive • Durham, North Carolina 27713
rone: (919) 544-5729 • Fax: (919) 544-5491
Printed: 17:42 09/14/97
35
-------
Page No.
09 14/97
Listing of S975864B.dbf
Hatched GC Peaks / Ratio / ReC. Time
Compound/
M_Z.... QC.Log Omit •.-.'hy . .RT. OK Ratio Total.Area... Area.Peak. 1.. Area. Peak. 2. . Rel. RT Con= =und.Name. . ID.. Flags.
356-358
13C12-PeCDD
368-370
368-370
HxCDF
374-376
D
D
374-376
13C12-HXCDF
384-386
384-386
HxCDD
390-392
D
DC :•!»
4
DC NL
DC SN
4
DC NL
d SN
DC SN
DC SN
d SN
DC SN
DC SN
6
27:40
Peaks
0:00
25:27
25:39
26:13
26:44
26:52
Peaks
0:00
28:12
28:21
28:39
28:49
29:11
29:16
29:22
29:36
29:46
30:27
30:33
30:38
Peaks
RO 2.61 0.97
33.53
1.32-1.78
RO 1.00 0.21
RO 2.73 3.16
RO 1.01 4.77
RO 4.16 14.31
1.48 3,079.17
1.53 269.84
3,368.09
2
23
1,839
162
"fit* m^l l .
.90
.32
.82
.99
1.05-1.43
1.32 2.20
1
1
1
RO 0
1
1
1
RO 0
1
RO 0
1
RO 0
.13
.34
.23
.99
.25
.22
.26
.92
.18
.94
.07
.48
10.81
23.59
5.75
3.20
40.06
17.32
5.15
7.33
23.53
3.40
8.69
0.54
124.00
5
13
22
9
.73
.52
.27
.S3
1.035
0.850-1.150
0.000
0.952
2.86 0.959
5.61 0.981
1,239.35 1.000 13ClC-PeCDD 123
106.85 1.005
I S3
0.959-1.050
0.000
5.08
10.07
17.79
7.79
0.
0.
0.
0.
0.
1.
1.
964
969
979
985
997 123478-HxCDP
000 123678-HxCDF
003
AH
All
1.011
12
4
.73
.50
0.43-0.59
DC NL
DC SN
6
0:00
28:11
28:20
29:10
29:16
29:46
29:53
30:28
Peaks
RO 0
RO 0
0
0
0
0
0
0
.78
.92
.50
.51 4
.51 4
.50 3
.54
.51 3
16
2.64
7.23
25.63
,188.09
,653.33
,937.59
4.56
,926.39
,738.26
UuS*fM9 t "--
1.05-1.43
DC NL
DC SN
d SN
DC SN
DC SN
DC SN
0:00
28:38
28:43
29:10
29:22
29:29
29:45
29:54
RO 0
RO 0
1
1
1
RO 0
1
RO 0
.74
.40
.06
.39
.25
.31
.40
.83
1.32
0.52
6.20
34.81
15.31
0.69
4.83
3.69
4
a
1.409
1,563
1.315
1.322
.39
.56
.02
.55
.35
.93
10.80
4.19
0.
4.79
17.07
2,779.07
3,089.78
2,622.24
2.603.46
1.
1.
1.
1.
017 234678-HXCEF
040
044
047
IB
863-1.137
0.
0.
0.
0.
1.
1.
1.
1.
000
963
968
997 13C12-HXOJF 478
000 13C12-HXCDF 678
017 13C12-HXCDF 234
021
041 13C12-HXCDF 789
SOR3
IS4
ALT2
ALT1
f*nn 0sil 1 i**t^«!
20
8
.22
.51
0.
14.59
953-
0.
0.
0.
0.
6.80 0.
0.
0.
0.
1.014
000
956
958
973
980
984
993
998 123478-HxCDD
AN
Triangle Laboratories, Inc.® Analytical Services Division
801 Capitals Drive • Durham, North Carolina 27713
Phone: (919) 544-5729 • Fax: (919) 544-5491
Printed: 17:42 09/14/97
36
-------
Listing of S975864B.dbf
Hatched GC Peaks / Ratio •'
Ret. Time
ipound/
;.. .. OC.Log Omit Why
.RT. OK Ratio Total.Area... Area.Peak.1. . Area.Peak.2.. Rel.RT Compound.Name.. I:.. Flags
D d SN 29:58
DC SN 30:03
D d SN 30:15
DC WH 30:40
2 Peaks
CCDD
DC NL 0:00
29:23
29:53
29:58
30:15
4 Peaks
RO 1.50
RO 0.57
RO 1.00
RO 0.68
1.05-1.43
RO 1
1
1
1
1
.68
.20
.21
.23
.22
»l*..»u.
8.27
0.81
a. oo
1.07
50.12
1.000 123678-HXCDD
1.006
1.009 123789-HxCDD
1.023
0.967-1.033
3.18
21.19
3.018
3.463
4.165
10,668
1 1. w»rv
.32
.09
.65
.25
n I
0.88-1.20
DC NL 0:00
31:55
32:08
32:15
D d nh 32:26
DC SN 32:50
M 33:06
DC WH 33:23
DC WH 33:35
4 Peaks
RO 0
1
0
RO 0
RO 1
RO 2
1
1
RO 1
.73
.12
.95
.79
.66
.45
.14
.05
.29
2
51
15
18
5
1
12
0
3
97
.10
.95
.04
.32
.37
.67
.40
.88
.10
.71
11
1,655
1,908
2.290
.58
.53
.78
.18
9.
1.362.
1,554.
1,875.
61
79
31
47
0
0
0
1
1
.000
.981
.997 13C12-HXCDD 478
.000 13C12-HXCDD 678
.009 13C12-HXCDD 789
A::
SUR4
IS5
RS2
27
7
9
6
.50
.32
.34
.60
24.
7.
11.
5
pCDF 0.37-0.51
DC NL 0:00
31:54
32:05
32:15
32:19
33:05
5 Peaks
RO 1
0
RO 0
0
0
0
.31
.44
.30
.46
.39
.41
1
2,668
8
22
18
2.205
4,923
.44
.37
.28
.93
.35
.62
.55
811
2
7
5
645
.03
.53
.19
.19
.09
1,857
8
15
13
1,560
0.995-1.042
.45
.72
.76
.80
0.
.34
.41
.74
.16
.53
0
1
1
1
1
1
1
1
1
937
0
1
1
1
1
1
.000
.001 1234678-HpCDF
.007
.011
.017
.029
.038 1234789-HpCDF
.046
.053
-1.125
.000
.000 13C12-HpCDF 678
.006
.011
.013
.037 13C12-HpCDF 789
AN
AN
IS6
SUR5
Above: HpCDF / IfcCDD Follows
0.88-1.20
DC NL 0:00 RO
M 32:09
D d nh 32:17 RO
M 32:45
DC WH 33:05 RO
2 Peaks
DC
NL 0:00 RO
32:09 RO
32:44
2 Peaks
1.88
1.14
1.76
1.08
1.63
18-1.20
0.61
1.28
1.02
1
18
8
25
4
44
2
26
2.884
2,910
.49
.75
.51
.60
.06
.35
.37
.07
.79
.86
10.00
13.30
16.32
1,457.94
0.977-1.005
0.000
8.75 0.982
0.986
12.30 1.001 1234678-HpCDD
1.011
AN
0.969-1.031
0.000
12.78 0.982
1,426.85 1.000 13C12-HpCDD 678 IS7
ingle Laboratories, Inc.® Analytical Services Division
Caprtola Drive • Durham, North Carolina 27713
ne: (919) 544-5729 • Fax: (919) 544-5491
Printed:! 7:42
-------
Page No.
09/14/9^
Listing of S975864B.dbf
Hacched GC Peaks < Ratio
/ Rec. Time
Compound'
M_Z.... QC.Log Omit Why ..RT. OK Ratio Total .Area... Area.Pea*.1. . Area.Peak.2. . Rel.RT Compound.Name.. ID.. Flags.
OCDF
442-444
442-444
0.76-1.02
DC
DC
DC
DC
DC
DC
DC
DC
DC
NL
SN
SN
SN
SN
SN
SN
SN
SN
1
0:00
31:50
32:07
32:18
33:40
33:55
33:58
34:23
34:52
35:25
Peak
RO
RO
RO
RO
RO
RO
RO
0.
0.
1.
3.
1.
1.
0.
1.
0.
0.
88
37
05
65
03
38
80
12
10
88
Above: HpCDD / Octa-CDD and CDF Follows
1.24
0.89
1.98
0.59
1.97
1.23
1.42
1.30
2.06
18.00 1.44 >.M
18.00
WT7-1.113
0.000
0.902
0.910
0.915
0.954
0.961
0.963
0.974
0.988
1.004 OCDF
OCDD 0.76-1.02
458-460 DC NL 0:00 RO 0.19 0.28
M 35:18 0.93 16.45
DC SN 35:39 RO 0.52 0.91
458-460 1 Peak 16.45
13C12-OCDD 0.76-1.02
470-472 DC NL 0:00 0.92 0.25
35:17 0.92 2,916.93
470-472 1 Peak 2.916.92
0.887-1.113
0.000
7.91 8.54 1.000 OCDD
1.010
0.996-1.DOS
0.000
1,399.27 1,3X7.65 1.000 13C12-OCDD
Column Description.
•Why" Code Description OC Log Desc.
M_Z -Nominal Ion Mass(es)
..RT. -Retention Time (mm:ss)
Rat.l -Ratio of M/M+2 Ions
OX -ROsRatio Outside Limits
Rel.RT-Relative Retention Time
End of Report
HL-Below Retention Tim* Window
WH-Above Retention Tia» Window
SN-Below Signal to Noia« Level
-------
Tilt:S975864 #1-905 Acqsl3-SXP-1997 00(14(42 EH- Voltag* SIS 70S Boim*»80
303.9016 r,2 BSOB(256,30,-3.0) PKD(9,S,5,O.OS\,320.0,1.00\,T,T) XxpiXPCOS
TBI ANGLE LABS TextlTLI M23 BLANK TLH43 057X1 IXT. TIME - 00(17
1001 A6.50E4
so:
19(00 20(00 21(00 22(00 23(00
rll«iS975864 #1-905 Aoq:13-SEP-1997 00(14(42 EI+ Voltag* SIX 70S Hoim*i253
305.8987 Ti2 BSUB(256,30,-3.0) PKD(9,5,5,0.05\,1012.0,1.00\,T,T) XzptEPCUS
TXIA1KLX LABS TuxttTLI M23 BLANK TLIt43057Xl UV. TIMX - 00(17
1001 A8.32S4
-1.3X4
C275K3—
0X0
Tim*
19:00 20:00 21(00 22(00
ril»:S975864 #1-905 Acq: 13-3EP-1997 00(14(42 EH- Voltage SIX 70S Nairn*1292
315.9419 Ts2 BSUB(256,30,-3.0) PXD(9,5,5,0.05\,1168.0,1.00\,r,T) XxpiXPCOS
TXIASGLX LABS TfXtlTLI M23 BLANK TLIM3 057X1 XK7. TIMX • 00(17
1001 A2.57Z7
ao:
60:
40:
20:
23(00
oJ
0.
19(00 20(00 21(00 22(00 23(00
Til»:S975864 #1-905 Acq:13-SEP-1997 00(14(42 EH- VoltMgu SIX 70S Moi*»:320
317.9389 Ti2 BSVB(256,3Q,-3.0) PXD(9,5,5,0.051,1280.0,1.00\,r,T) XxpiXPCOS
TRIANGLE LABS TtxtiTLI M23 BLANK TLII43057X1 OfT. TIMX » 00(17
1001 A3.32X7
80:
60:
40:
19(00 20(00 21(00 22(00 23:00
Til»tS975864 #1-905 Acqt 13-SEP-1997 00(14(42 EH- Voltagw SIS 705
330.9792 Fs2 XxptXPCOS
TRIANGLE LABS TarttTLI M23 BLANK TLH43057X1 XHET. TIME " 00(17
1001, 18(57 19(19 . _ 30,41 _31t22^ 21t4t 22(45
^*S\f* * Afc^ »*A
80;
60:
40:
20:
19(00 20(00 21(00 22:00
rll*iS975864 #1-905 Aojil3-SEP-1997 00(14(42 EI+ Volt*g» SIX 70S
375.8364 Ti2 XxpiXPCOS
TRIANGLE LABS TmxtiTLI M23 BLANK TLIM3057X1 OKT. TXMX •
1001 21 51
80:
60:
23(00
.7X6
.2X6
,6X6
.1X6
.5X6
0X0
Urn*
.0X7
,0X6
,0X6
.0X6
.0X6
.0X0
Hm*\
,0X7
.4X6
,3X6
.2X6
.1X6
.0X0
Hm*\
00(17
40.
20:
18,57
19,29
7 *•'•— 20(47 I 23(03
x^J^teiJOLku^^
jOUt»
19(00
20(00
21(00
22(00
23(00
4*4
1X4
4X3
6X3
8X3
.0X0
Tim*\
39
-------
r±l»,S975S64 il-905 Aoqtl3-SXP-1997 00*14*43 ZZ+ Voltfgm SIS 70S Wo±**,86
319.8965 r>2 BSUB(256, 30, -3.0) PXD(7,5, 3,0. 05\, 344.0,1.00%, r,T) XxptXPCUS
TRIANGLE IMS TextiZXJ M23 BLANK IXJMJ057BJ, . OKT. TOOf - 00tl7
20100 21,00 22tOO 23*00
TilmtS973864 #1-905 Acqsl3-BEP-1997 00tl4t42 JET* Voltage SXt 70S maim*177
321.8936 Ft2 BSVB(25S,30,-3.0) PXD(7,5,3,0.051,308.0,1.00\,r,T) XxptXPCOS
TXIAHBLX LASS TeitjUJ N33 BiAMT ZZJMJ057JU 2X7. ZZXK - 00(17
A3.29X4
20100 21', 00 22', 00 23', 00
ril»,S975B64 il-905 Aoqtl3-BSP-1997 00,14,42 XI* Volt»g» SIS 70S Hoimmt647
331.9368 r>2 *Stn(2S6,30,-3.0) PXD(7,5,3,0.05\,2388.0,1.00\,r,T) XxptXTCUS
TXXANGLX LASS T*zt>Z£T M23 BLANK TLIt43057Rl JMJ. TOO • 00<17
-,_
1X4
8E3
6X3
4*3
0X0
2ttMJ
1001
Aj.imM/
8AI.MI7
ni
It 1
_O. VfP
.4.8X6
J.tMf
20,00 21,00 23,00 23,00
ril»,8975864 il-905 Aoqil3-BXP-1997 00tl4l42 JEI* Volttgm SIX 70S Ht>iMmt30f
333.9338 tt2 iSUg(256,30,-3.0) PKD(7,5,3,0.05\,»24.0,1.00\,r,T) XxptXPCOS
XXIAMSLX LASS TmittTLI M23 BLANK TLH43057X1 OKT. TOO - 00.17
1001
00:
60.
40:
20:
ol
.34X7
20100 21,00 22,00 23,00
rll»,S975864 #1-905 Actj,13-SKP-1997 00,14,42 XH- Voltmgm SIX 70S Waifu,213
327.8847 Ti2 *Stn(25£,30,-3.0) PKD(7,S,3,0.05\,852.0,1.00\,TrT) XxptXPCOS
XXIANGLX LABS TarttTLI H23 BLANK TLI443057X1 UKT. XXKK - 00>17
1001 A3.68X7
80:
sol
40l
sol
OJ
20,00 21100 22,00 23,00
ril»iS975864 41-905 Aoqtl3-SXP-1997 00tl4i42 ZI+ Volt»gm SIX 70S
330.9792 r,2 XxpiXPCUS
IXIAJKLX LABS TflttTLI H23 BLANK TLH43057X1 OKT. TOtX - 00tl7
100* 19,50 20107 20123 2014120156 31,22^ 21,48 22i04 .2*1*6
40:
20:
o.
23,25
-7
.6.
.4.
,3.
6X6
1X6
5X6
0X6
5X6
0X0
.0.
.6.
.4.
.2.
20,00
21,00
22,00
23,00
7X6
5X6
4X6
2X6
.0X0
Tim*
.0X7
.2X6
2X6
1X6
1X6
0X0
TlmJ
40
-------
rile:S975864 il-905 Aoqtl3-SEP-1997 00tl4i42 EI+ Voltagw SIS 70S mo±mmi9t
339.8597 Tt2 BSUB(256,30,-3.0) PKD(7,5,3,0.05\r392.0,1.00\,rrT) ExptEPCOS
TRIANGLE LABS TmxtiTLI H23 BLANK TLH430S7X1 OtT. TUB - 00»17
24100 25100 26100
rile,3975864 fl-905 Acqtl3-8XP-1997 00,14,42 EI+ Voltag* SIX 70S Mo±m»tl69
341.8567 r,2 BSVB(256r30r-3.0) PKD(7,5,3,0.05\,676.0,1.00\,r,T) XxptXPCOS
TSIAtfSLE LABS TmztiTLI M23 BLANK TLIf43057Xl ZK7. TIME - 00>17
A4.80E4
27:00
24100 25 tOO 26100
ril»tS975864 fl-905 Aoq>13-SXP-1997 00,14,42 EI+ Volt*g» SIX 70S Boif9t71
351.9000 Tt2 BSVB(256,30,-3.0) PXD(7,5,3,0.05\,284.0,1.00\,T,T) XxptXPCOS
TSIJOfSLE LABS TmxttXLX H23 BLANK SLH43057X1 XK7. ZZMB - 00il7
100\
27100
so:
20:
A2.53X7
24,00 25i00 26i00 27tOO
rile,3975864 fl-905 Acqtl3-SEP-1997 00,14,42 EH- Voltage SIX 708 Mol*»,83
353.8970 Tt2 BSUB(256,30,-3.0) tKD(7,5,3,0.05\,332.0,1.00\,T,T) KxptEPCUS
TRIANGLE LABS T*xt,TLI M23 BLANK TLIt43057Xl BKT. TIME - 00,17
1001 A2.Q8E7
80:
50:
40:
20:
0.
24,00 25i00 26,00 27,00
Tile,S97S864 tl-905 Acgil3-SXP-1997 00,14,42 11+ Voltage SIX 70S
330.9792 Fi2 ExpifPCUS
TRIANGLE LABS TextsTLI M23 BLANK TLH43057R1 HKT. ZZXT - 00<17
23,53 24,16 _ «i«_. . _2S^15 25^3525^2^,08
24,00 25100 26', 00
rilm,S975864 tl-905 Acg, 13-SEP-1997 00,14,42 III- Voltagm SIX 70S
409.7974 T,2 XxpifPCOS
TRIANGLE LABS TfjctiTLI M23 BLANK XLH43057X1 OKT. TIME •
lOOi
80:
27100
.9.7X6
.7.3X6
.5.8X6
.3.9X6
.1.9X6
0.0X0
Tim*
6.7X6
.5.4X6
.4.0X6
.2.7X6
.1.3E6
0.0X0
24100
25100
26,00
27:00
41
-------
fm>tS975864 tl-905 AcqtJ.J-SET-1997 00,14,41 EI+ VOlCagr* SIX 70S MDlfm,i4
355.8546 Tt2 BSUB(256,30,-3.0) PKD(7,5,3,0.05\,316.0,1.00\,r,T) XzptXPCOS
TXIAHSLX LABS Text»IXX H23 BLANK TLIt43057X1 ZK7. TZMX - 00*17
1001 Al. 8X5
24*48 35,00 25*12 35,34 25*36 25*48 26*00 26*12 26*24 3ft36 26*48 27,09 27,12 27,24 27,36
Fil»,3975864 tl-905 Aoqil3-SXP-1997 00*14*42 XX* Voltugm SIX 70S Boif*>*52
357.8516 r,2 BSOB(256,30,-3.0) HO>(7,5,3,0.05\,208.0,1.00\,T,t) XxptXPCUS
TSIA1KLX LABS TertiXLI M23 BLANK TLI§43057X1 Off. TXHX - 00117
1001 A4.68C4
24,48 25*00 25*12 25*24 25*36 25*48 26,00 26*12 26*34 2ft36 36*48 27*00
rila,3975864 tl-905 Aoqtl3-SXP-1997 00*14*42 XI+ Volt*gm SXX 79S *>i»*t64
367.8949 T*2 BSVB(256,30,-3.0) PKD(7,5,3,0.03*r33*~*fJt.Sf*frtT) XXftSFCOS
100\ Al.l
80.
60.
40.
20.
27,24 27,36
24*48 25*00 25*12 25*24 25*36 35,48 26*00 26,12 26*24 2f*3S26i48 37',b'o' 37,13 37*34
ril»,S975864 tl-905 Aoq*13-SXP-1997 00*14*42 XH- Yoltmgm SIX 70S M>if9,65
369.8919 ft2 BSUB(256,30,-3.0) PXD(7,5,3,0.051,260.0,1.00\,r,T) XxptXPCOS
XXIAIKLX LABS TmxttXLI M23 BLANK XLIt43057Xl OOT. TUfX - 00,17
10n A1.24X7
80.
60.
40.
20.
0.
_5.<
.4.0X6
.2.7X6
.1.3X6
27t36
0.0X0
Tim*
^4.5X6
.3.6X6
.2.7X6
J..8X6
_9.0Z5
1.07S6
J\
24i48 25*00 25*12 25*24 25*36 25*48 26iOO 26*12 26*24 26*3626*48 27*0027*12 27*24
Fllu,3975864 tl-905 Aeqil3-SXT-1997 00*14*42 XI+ Volttyu SIX 70S
330.9792 T*2 XxpiXPCUS
TXIANSLX LABS TmxtiXLX M23 BLANK TLH43057X1 IMT. TTMX ' 00*17
ion
27*36
o.oxo
Tim*
34, 48 25i 25*12 25t24 25136 3548 2600
26*24 26*36 26,48 27*00 27,12 27,24 27,36
42
-------
Til**S975864 tl-346 Acq*13-SEP-1997 00*14*42 XI+ Voltage SIS 70S Noim*:624
373.8208 F*3 BSUB(256,30,-3.0) PXD( 7,5,3,0. 05\,2496. 0,1.00\,T,T) XxpiXTCUS
TRIANGLE LABS T*Xt*TLI M23 5ZJUOT TLIt43057Sl IKT. TIMX - 00*17
loot
80:
60:
40:
20:
A2.23E5
/I
A1.35E5 l\ A1.27X5
A A I
-9.1X4
U-Z3** \ \ \ \ A4.50X4
\f\J\ ^A3i£"^ .^J \J{^ Aj^'4/ W-^*3 -A
'.7.3X4
-.5.5X4
'.3.6X4
11.8X4
'•o.oxo
28*12 28*24 '28:36 28*48 29*66 29\'l2 2J»»ii 29*36 29*48 30': 00 36*12 36':24 36*36 3o':48 SltOO Tim*
ril**S975864 tl-346 Aoq*13-8XP-1997 00*14*42 XI+ Volt*?* SIS 70S Hoi** 1 474
375.8178 F*3 BSUB(256,30,-3.0) PXD(7,5,3,0.05\,1896.0,1.00\,r,T) XxpiXPCUS
TRIANGLE LABS T*It:TLI M23 BLAST TLIt43057Sl 1ST. TIME - 00.17
100J
80.
60:
40:
20:
A1.78XS
A1-01S5 A A1.08X5
A J\ A1.79X4 J\l\ V\
-1.9X5
A4.19X4
.1.5X5,
.1.1X5
.7.4X4
.3.7X4
.0.0X0
28'tl2 28': 24 28': 3 6 28*48 iiioo '29\12 29*24 29\36 29*48 30*66 30*12 3'o':24 3o't36 30.48 jiloO Tim*
ril**S975864 tl-346 Acq*13-8Xf-1997 00*14*42 EH- Voltug* SIS 70S Hoi** t 6 82
383.8639 T*3 BSVB(256,30,-3.0) PXD(7,S,3,0.05\,2728.0,1.00\,T,X) XxptXPCDS
TRIANGLE LABS T*It:TLI M23 BLAmf XLIt43057Sl XKT. TIMX - 00.17
1001
80:
60:
40:
20.
o:
** I6*7 U.32X7
A ft 1
1 \J \ ) \
A1.32X7
I
'
1 \
-6.0X6
.4.8X6
.3.6X6
.2.4X6
.1.2X6
0.0X0
28:12 28*24 28*36 28*48 29*66 ' 29*12' 29* 24 29* 36 ' 29*48 ' 30*66 ' JOili' 30\24 ' 30* 36' 30*48 ' 31i6o Tim*
ril**S975864 tl-346 Acq*13-SXP-1997 00*14*42 EH- Volt*g* SIS 70S Sol*** 87 5
385.8610 Ti3 BSUB(256 ,30, -3.0) TXO(7,5,3,Q.05\,3500.0,l.OO\trrT) XxpiXtCUS
TRIAHStX EJIBS T^l-tiTtT JT3J BTJUIT •n^T»43O57Sl TUT. TTU
1003
sol
sol
40:
20:
o:
v - no, 17
^99X7 ^6m ^.2X7
A A I
J \J \ J \
»
/ V
J.7X6
.7.3X6
.4.8X6
.2.4X6
O.OXO
28*12 28*24 28*36 28*48 29': 00 29': 12 29*24 29'i36 29\48 3o'*66 30:12 30:24 30:36 30*48 31\00 Tim*
Til**S975864 tl-346 Aaq*13-SXf-1997 00*14*42 EH- Voltay* SIS 70S
392.9760 T*3 XxpiXTCUS
TRIANGLE LABS T*rt*XLI M23 BLAKf TLH430S7S1 ItKT. TIMX - 00*17
1001
80:
60:
40:
20:
o:
28*07 38*25 28*45 29*03 29*17 39,39 ia.*t 30*22 30*33 . 30.55
(Vv^vAv^^^\A-^^
f
-5.6X6
.4.5X6
.3.3X6
.2.2X6
•J..1X6
• O.OfO
28*12 28*24 28*36 28*48 29*66 29:12 29*24 29*36 29*48 JOi 00 ' 36*12' 36'i24' 3o'i 36 ' Jbiis ' JlioO Ttm*
ril**S975864 tl-346 Aoq*13-SXP-1997 00*14*42 XI+ Voltmg* SIS 70S
445.7555 Ti3 XxpiXPCVS
TRIANGLE LABS T*Xt.:TLI M23 BLAtOt XLIt43057Sl XKT. TIMX " 00*17
1001
80:
60:
40:
3rt •
"
oj
1
C2.1X4
I 39*30 30 04 3Qt46
n 28,40 1 39*53
\\28ill 1 28:33 1 29:10 1 111
llT A IT ML A. * Ml . 1 . -»Al » lid A An A A 1
I1»_AJL -,-J»U <_.-i. |WAJ«^ft ^ ^^ ^r,n/^/\A ,fr, fAfit-, /""S,, iV^A/Ai/\llvV7l-_l
30*35 1
1 130*21 . .All .1 /t.
» — A-^v^^AAAJl/vvLAwJUArf^AA.
J. 7X4
IJ..3X4
.8.4X3
.4.2X3
28:12 28*24 28*36 28*48 29*66 29': 12 29*24 29*36 29*48 36*66' 30*12' JOiii' 30* 36 ' 30*48 ' 31t6o Tim*
43
-------
piO.«JS»7586« tl-346 AoqtJ.J-SSP-J.997 00,14,42 EI+ VoJ-tMyf SIS 70S HO1**,J66
389.8156 Ti3 BSUB(356r30,-3.0) PKD(7,5,3,0.05\,1464.0,1.00\,T,T) XxptXPCUS
TRIANGLE LASS TfXttXLI M23 BLAKK TLIt4 3057X1 UKT. 1TMT - 00il7
1001 A2.02E5
80.
60.
28:36 28,48 29,00 29,12 29,24 29,36 29i4l 30,00 30,12
rilmiS975864 tl-346 Aaq,13-SXP-1997 00tl4>42 XX+ Voltaym SOt 798 Hol*»>490
391.8127 r,3 BSUB(356,30,-3.0) PKD(7, 5,3,0.05\,1960.0,1.Ot\,T,T) XxplXfCDS
TSIASSLX LABS TtortiZZJ M23 BLAXK TLIt4 3057X1 OCT. TXM* - 00>17
100\ A1.46K5
80.
60.
40.
40.
20.
A3.19E4
•¥
A
^^^^^
MS.54X4
A4.43X4
30,34
30136
At. 80X4
Alt 3304
A3.69*4
-9.2X4
.7.4X4
J.5X4
^3.7X4
.1.8X4
0.0X0
Time
-6.2X4
.4.9X4
.3.7X4
-2.5*4
20.
A3.01X4
A3. AIM
.1.2X4
o;
28', 36 28,48 29,00 29,12 29', 24 29,36 29', 48 30,00 30*12 30,24 30*36
Tile,3975864 tl-346 Aoq*13-SXP-1997 00,14,42 XH- Voltagm MIX 70S Ho±M*ill88
401.8558 r,3 BSUB(256,30,-3.0) PKD(7,5,3,0.05\,47&2.0ti.^»%fT,S) f-f-mmm
TRIANGLE LABS 2tezt>2ZJ M23 BLABS TLIt43057Xl OO. SOB - 90,17
loo* a2
00:
60.
40.
20:
0
, , I, . > / , .
28,36 28,48 29,00 29,12 29,24 29,36 29,48 30,M 30,12 30,24 30t36
Tile,3975864 tl-346 Acq,13-SXP-1997 00,14,42 XT-f Voltrym SIX 70S maim»,712
403.8529 T,3 BSUS(256,30, -3.0) PKD(7,5,3,0.05\,2848.0,1.00\,T,T) XxptXPCUS
XSIANGLX LASS TmrttXLX M23 SLAKK XLIt43057Xl XK7. TTHT - 00*17
100\ A1.88X7
A1.55X7
so:
60L
40.
20:
A1.36X.
28t36 28,48 29,00 29,12 29,24 29,36 29,48 30,00 30,12 30,24 30*36
rlleiS975864 tl-346 Aoqt 13-8XT-1997 00,14,42 KI+ Voltay* SIX 70S
392.9760 Fi3 XxpiXPCOS
TBIANSUS LABS TvrtiTLI H23 BLANK TLH43057X1 ZK7. XTMK • 00,17
1001
80.
60.
40.
20.
0.
28145
29103
29,26
},35
29157
30,14 30,22 _ 39f33
29, 41
0*0
Ximm
.7.4X9
.5.6X6
.3.7X6
.1.9X6
0.0X0
T±m*
.7.6X6
.6.0X6
.4.5X6
.3.0X6
.1.5X6
0.0X0
.5.6X6
.4.5X6
.3.3X6
.2.2X6
.1.1X6
0.0X0
28,36 28,48 29,00 29,12 29,24 29,36 29,48 30,00 30,12 30,24 30,36
44
-------
rila,S975864 41-390 Aoqtl3-SXP-1997 00il4i42 XH- Volttym SIX 70S Noifm,533
407.7818 f,4 BSOB(256,30,-3.0) PKD(7,5,3,0.05\,2132.0,1.00\,r,T) XxptXPCOS
TXIANSLX LABS TaxttTLI M23 BLANK TLH43057S1 ZK7. TIMX - 00il7
1001 A3.75X5
00:
60:
40:
201
A9.34E4
A7.32X4
AS.40X4
A4.37X4
A2.01E4
.94X3 A4.54X3
/\ ^xv .-.
Jl«48 32,00 32:12 32:24 32,36 32:48 33,00 33,12
,3975864 tl-390 Acq,13-SXP-1997 00,14,42 XH- Voltay* SIX 70S Jtoi*9,730
409.7.789 F,4 B8UB(256,30, -3.0) PXD(7,5,3,0.05\,2920.0,1.00\,r,T) XrptXPOJS
TXIAJKLX LABS TmxttTLI M23 BLANK TLIt43057Sl IHT. TIMX - 00<17
1001 A2.15K5
80:
33,24
60:
40:
20:
A1.65.
A1.18XS
^.72X4 /U
^y\y VAJ£rgg
.63X4
32,00 ' ' ' 32tl2 ' ' ' 32,24 ' ' ' 32,36 32:48 33iOO 33tl2
rile,3975864 tl-390 Acqil3-SXP-1997 00,14,42 XH- Voltage SIS 70S Soif»,656
417.8253 F:4 BSUB(256,30, -3.0) PXD(7,5,3,0.05\,2624.0,1.00\,T,T) XxptXPCUS
TRIANGLE LABS TtxttTLI M23 BLANK TLIf43057Sl OfT. TIMX - 00tl7
1001 A8.J.1X6
33,24
80:
60:
40:
20:
oj
A6.45X6
31:48 32,00 32:12 32:24 32,36 32:48
Tile,S97S864 tl-390 Aoq,13-SXP-1997 00,14,42 XH- Voltage SIS 70S
419.8220 F,4 BSVB(256,30,-3.0) PXD(7,5,3,0.05\,1992.0,1.00\,T,X)
TXIAJKLX LABS TexttTLI M23 BLANK TLIt43057Xl HOT.
1001 A1.$6X7
80:
50:
40:
20:
o:
33,00 33:12
SolM»,498
XrptXPCOS
TIMX - 00>17
A1.56X7
31,54
31:48 32:00 32:12 32,24 32,36 32:48 33,00 33,12
,3975864 tl-390 Aog,13-SXP-1997 00:14,42 XII- Voltag* SIS 70S
430.9729 r,4 XxptXPCOS
TXIAJKLX LABS TextsTLI M23 BLANK TLIt43057Ml HKT. TIMX - 00,17
32,31 32,38
32t07
32,24,
S0j
40:
20:
0:
33,24
31:48 32:00 32:12 32:24 32,36 32:48
r±l»,3975864 tl-390 Aoqil3-SXf-1997 00,14,42 XH- Voltage SIS 70S
479.7165 F,4 XxfiXICUS
TXIAJKLX LABS T»xt>TLI M23 BLANK TLIt43057Xl HKT. TIMX - 00>17
1001 32;12
80:
60:
40:
201
33:24
o
33106
31:56
31,48
32,00
32:12
32,24
32,36
32,48
33:00 33112
.8.8X4
-.7.1X4
.5.3X4
.3.5X4
.1.8X4
0.0X0
^9.8X4
.7.8X4
.5.9X4
.3.9X4
.2.0X4
.0.0X0
21**
,3.3X6
.2.7X6
J.OX6
.1.3X6
.6.6X5
o.oxo
-7.7X6
.6.2X6
.4.6X6
.3.1X6
.1.5X6
0.0X0
^4.0X6
.3.2X6
.2.4X6
.1.6X6
.7.9X5
0.0X0
-1.8X4
.1.4X4
.1.1X4
.7.2X3
.3.6X3
0.0X0
33124
-------
Fil»:SS758t4 tl-390 Acq:13-SEP-lS37 00:14:41 EI+ VoXtacf* SIR 70S Half*, 6 83
423.7766 Tt4 BSOB(256,30,-3.0) PKD(7, 5,3,0. 05\,2732. 0,1. 00\,r,T) Xxp:XPCUS
TRIANGLE LABS TmxtsTLI H23 BLANK TLII43057X1 UfT. TIHX " 00,17
1001
BO.
60.
40.
20.
A1.46XS
l\
A
A1.41E5 I \
/ \ 11
/ \ 11 A3.25E4
/v^ VV^A^^ I ^ „ ^A
-5.7X4
.4.5X4
.3.4X4
.2.3X4
.1.1X4
3'2>66 32:06 32:12 32:18 32:24 32', 30 32', 3 6 '32:42 32', 4 8 32', 54 33', 66 33', 06 33 ',12 Timm
rllm:S975864 41-390 Acqtl3-SXP-1997 00,14,42 XI+ Volt*gm SIX 70S Woifm,364
425.7737 F:4 BSOB(2S6,30,-3.0) PKD(7, 5, 3, 0.05\, 1456.0,1 .00\,T,T) XipiEPCUS
TRIANGLE LABS TextilZJ H23 BLANK TLH43057X1 JKT. TIHX - 00:17
1001
BO:
60.
40:
20:
A1.33X5
A1.03E5
A
\
\
-4.8X4
.3.8X4
.2.9X4
.1.9X4
.9.6X3
32:66 32:06 32:12 32:18 '32:24 32:36 32:36 '32:42 32:48 '32:54 '33:66 33:06 33:12 Timm
rllm:S975864 91-390 Aoq:13-SXP-1997 00:14:42 XI+ Voltugm SIX 70S Xolmmt606
435.8169 r:4 BSUB(256,30,-3.0) PKD(7,5,3,0.05\,2424 ,0,J..OO\,T,T) Ezp:XPCUS
TRIANGLE LABS Text. IX J H23 BLANK TLH43057R1 TXT. TIHX - 00»17
1003
so:
eo:
40:
20:
o:
A1.46X7
\
A
/ \
y v
-6.3X6
.5.0X6
.3.8X6
.2.5X6
.1.3X6
0.0X0
32:66 32:06 '32:12 '32:18 '32:24 32': 30 32:36 '32:42 32:48 32:54 33:66 33:06 33:12 Time
rila:S975864 H-390 Aoq:13-SEP-1997 00:14:42 XI+ Voltage SIR 70S So±t»,9B9
437.8140 F:4 BSOB(256,30,-3.0) PKD(7r5, 3,0. 05\f 3956. 0,1. 00\,r,T) XxptXfCUS
TRIANGLE LABS Text .-1X1 M23 BLANK TLH43057R1 ZK7. TIME - 00»17
1001
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n
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430.9729 T:4 Xxp:XfCUS
TRIANGLE LABS T«Xt<2XI M23 SLANK TLH43057R1 HKT. TIHX • 00>17
1001
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32:31 32:38 /-V^/^X1?1 /ty^~
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.2.3X6
.1.6X6
.7.BX5
0.0X0
1 Timm
46
-------
nia:SS75864 tl-390 AdjtI3-SXP-1997 00,14,42 EH- VoltMg* SIM 70S Boimm,288
441.7428 T:4 BSUBf 256,30,-3.0) PKD(7,5,3,0.05\,1152.0,1.00\,r,T) txptXPCOS
TXIAXGLS LABS Text:Til H23 BLANK TLIt43057Xl OST. TIME - 00:17
1003)
80j
70j
SOj
401
3ol
201
101
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513.6775 r,4 ExptEPCUS
TXIAtKLX LABS TaztilZJ M33 BLANK TLH43057X1 HCJ. TIHX -
1004
00:17
rJ.5£4
.3.1X4
.2.8X4
.2.4X4
.2.1X4
.1. 7X4
.1. 4X4
.1.0X4
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.3.5X3
.0.0X0
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-.0.0X0
Time
-4.1X6
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.2.9X6
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.1.2X6
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0.0X0
47
-------
fiJ.e,SS/5B64 tl-JSO AcqtJ.J-SEP-J.S97 00,14,43 EI+ VoJ.f*f» SIX 70S KolS*l67
457.7377 r,4 BSUB(256,30, -3.0) PKD(7,5,3,0.05\,268.0,1.00\,T,T) XzptXPCOS
TRIANGLE LABS Text>XLJ H23 BLANK TLII43057X1 HK7. XIHX - 00:17
100% A8.63X4
35112 35', 18 35', 24 35', 30 35,36
rile,S975864 tl-390 Aoqtl3-8XP-1997 00,14,42 XI+ Voltag* SIM 70S Holme,351
459.7348 Tt4 BSVB(256,30, -3.0) PXD(7,5,3,0.05\,1404.0,1.00\,r,X) XxptXPCUS
XSIANGLX LABS TfJCttTLI M23 BLASX TLH43057X1 EC7. TOOS - 00.17
J 00* AJ.J
A7.19K3
A4.35I3
-3.0E4
-2.4X4
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35,12 35,18 35,24 35,30 35,36
r±l»,S975864 tl-390 Acgil3-BXP-1997 00,14,42 XH- VoltMgm SIX 70S Solf»i62
469.7779 Tt4 3SO*(256,30,-3.0) PXD<7,5,3,0.051,248.0,1.00\,T,X) XxptXTCOS
TXIANGLX LABS TmxtiTLI H23 BLANK TLIt43057JU OUT. IXHX - 00(17
1001 A1.40X7
80.
60.
40.
20.
35,42
35,12 35,18 35,24 35,30 35,36
rilf,S97SB64 tl-390 Acqtl3-SEP-1997 00,14,42 EI+ Voltug* SIX 70S Hoi»»t65
471.7750 r,4 BSUB(256,30,-3.0) PXD(7,5,3,0.05\,260.0,1.00\,r,T) XxpiXPCUS
TXIANGLX LABS TttIt:TLI M23 BLANK TLIt43057Rl UKT. XXMX - 00<17
1001 A1.5.2X7
801
so:
40:
20:
35142
35,12 35,18 35,24
r±lmiS975864 tl-390 Acqil3-SXP-1997 00,14,42 XI+
430.9729 r,4 XxpiXPCUS
TSIA1KLX LABS T*xt,TLI H23 BLANK XLIt43057Xl
1001
35,30
SIX 70S
35,36
35,42
.0.0X0
Tim*
5.3X6
4.3X6
.3.2X6
.2.1X6
.1.1X6
.0.0X0
Tim*
.5.7X6
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.3.4X6
.2.3X6
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801
601
401
201
01
35,13
35*44
35:12
35:18
35124
35,30
35t36
35,42
.4.1X6
'.3.3X6
.2.5X6
.1.7X6
.8.3X5
0.0X0
48
-------
File:S975864 #1-905 Acq:13-SEP-1997 00:14:42 EI+ Voltage SIR 70S
339.8597 F:2 Exp:EPCUS
Sample Text:TLI M23 BLANK TLI#43057Rl INJ. TIME =
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341.8567 F:2 Exp:EPCUS
Sample Text:TLI M23 BLANK TLI#43057R1 INJ. TIME =
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375.8178 F:3 Exp:EPCUS
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409.7789 F:4 Exp:EPCUS
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417.8253 F:4 Exp:EPCUS
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471.7750 F:4 Exp:EPCUS
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File:S975864 #1-390 Acq:13-SEP-1997 00:14:42 EI+ Voltage SIR 70S
459.7348 F:4 Exp:EPCUS
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Sample Text:TLI M23 BLANK TLI#43057Rl INJ. TIME =
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-------
TLI Project: 43057rl Method 23 TCDD/TCDF Analysis (DB-225)
Client Sample: TLI M23 Blank Analysis File: P973848
Client Project:
Sample Matrix:
TLI ID:
Sample Size:
Dry Weight:
GC Column:
| '"""'" ^
Analytest j
XAD
TLI Blank
1.000
n/a
DB-225
— T^M*
Date Received:
Date Extracted:
Date Analyzed:
Dilution Factor:
Blank File:
Analyst:
tta*^«gtt^
09/06/97
09/12/97
n/a
P973848
WK
^
Spike File:
ICal:
ConCal:
% Moisture:
% Lipid:
% Solids:
tf*:»*r*'tf!
SPC2NF04
PF22206
P973843
n/a
n/a
n/a
(T.. •-»*.
2,3,7,8-TCDF
ND
0.008
Internal St««iarel,
Amt
13C12-Z3,7,8-TCDF
2.9
72.7 40%-130%
0.76 20:40
Recovery Standard
'3C,2-1,2,3,4-TCDD
0.81 19:42
Data Reviewer
Page 1 of 1
Triangle Laboratories, Inc.*
801 Capitola Drive • Durham, North Carolina 27713
Phone: (919) 544-5729 • Fax: (919) 544-5491
09/14/97
C2NF.PSR »2.00. LARS 6.10.04
Printed:! 7:54 09/14/9V
-------
Initial
....Date...
aca Review By:
c ^/
Calculated Noise Area:
1.37
he Total Area for each peak with an ion abundance ratio outside
atio limits has been recalculated according to method requirements.
age No.
9/14/97
Listing of P973848B.dbf
Matched GC Peaks / Ratio / Ret. Time
ompound/
[_Z.... QC.Log Omit Why ..RT. OK Ratio Total.Area... Area.Peak.1. . Area.Peak.2.. Rel.RT Compound.Name.. ID.. Flags.
•CDF
104-306
S 04-3 06
1.86
2.18
1.01
0.53
0.44
0.83
1.34
1.72
0.00
0.786-1.096
0.000
0.938
0.979
0.981
0.984
1.008
1.010
1.019
13C12-TCDF
116-318
316-318
2.49
1.52
9.49
5.95
1,683.28
5.27
1.54
12.08
1.688.55
729.00
2.38
0.952-1.048
0.000
0.917
0.938
0.950
954.28 1.000 13C12-2378-TCDF ISO
2.89 1.026
1.047
1.090
Above: TCDF / TCDD Follows
13C12-TCDD
332-334
332-334
DC
DC
DC
DC
DC
DC
NL 0
SN 17
SN 18
19
19
20
WH 21
WH 21
WH 21
0.
:00 RO
: 32 RO
:26 RO
:28
:42
:22
:34 RO
:45 RO
:55
65-0.89
1.87
2.59
0
0
0
0
2
0
0
.39
.79
.81
.82
.58
.43
.80
3 Peaks
1
0
3
1,370
1,668
16
0
1
3
3,055
.72
.51
.56
.66 605.30
.46 744.76
.80 7.58
.58
.08
.76
.92
0.897
0
0
0
765.36 1
923.70 1
9.22 1
1
1
1
-1.103
.000
.901
.947
.000
.012
.046
.108
.117
.126
13C12-2378-TCDD IS1
13C12-1234-TCDD RSI
Triangle Laboratories, Inc.® Analytical Services Division
J01 Caprtola Drive • Durham, North Carolina 27713
3hone: (919) 544-5729 • Fax: (919) 544-5491
Printed: 17:54 09/14/37
-------
Page No. 2 Listing of P973-.43B.dbf -
09/14/9" Matched GC Peaks •' Ratio / Ret. Time
Compound,'
M_Z.... QC.Log Omit Why ..RT. OK Ratio Tctal.Area... Area.Peak.1.. Area.Peak.2.. Rel.RT Compound.Name.. ID.. Flags.
Column Description "Why" Code Description QC Log Desc.
M_2 -Nominal Ion Hassles) WL-Below Retention Time Window A-Peak Added
..RT. -Retention Time (nsnrss) HH-Above Retention Time Window K-Peak Kept
Rat.l -Ratio of M/M+2 Ions SN-Below Signal to Noise Level D-Peak Deleted
OK -RO=Ratio Outside Limits
-------
rjU.etF97.3840 tl-755 Aoq,12-SEP-lS97 151 Otis 10 EH- Voltagtt SIX TOP Noia*:J7J
303.9016 BSOB(256,30,-3.0) PJ3>(5,3,1, 0.10%, 1492.0,0.00\,T,r) XxptDB225
TRIANGLE LABS TaxtlTLI H23 BLAST TLIt43057Xl
100* AS.Q6X3
17.00 18.00 15,00 20,00 31,00
Tllf,P973848 tl-755 Acqtl2-8XP-1997 15,06,10 XI+ Volt*g* SIX 70P No±»»:556
305.8987 BSOB(256,30,-3.0) PXD(5,3,1,0.10\,3324.0,0.00\,f,P) Exp:DB235
TRIANGLE LABS TtxttZCJ H33 BLANK TLIt43057Xl
1001 A2.26E4 A1.34X4
80.
23:00
17:00 18.00 15.00 30.00
r±2«tP973848 91-755 Acqtl2-SXP-1997 15:06:10 XI+ Voltag* SIX 70P Koia»:5B6
315.9419 BSOB(25e,30,-3.0) PXD(S,3,1,0.10\,2344.0,0.00\,T,T) SxpiDB225
TRIANGLE LABS Text.ZXX H33 SLANT TLIf43057Xl
1004 A7.39K6
80.
60.
40.
20.
.1.5X6
.1.2X6
.7.7X5
.3.9X5
17:00 18:00 19:00 20:00 31:00
rlleiP973848 tl-755 Acqil2-SZP-1997 15:06,10 XH- Voltagm SIX 70P No±f9:660
317.9389 BSOS(256r30,-3.0) PXD(5, 3,1, 0.10\,3640.0,0.00\,T,T) ExptDB225
TRIANGLE LABS T(uct:TLI M23 BLANK TLIt430S7Sl
1004 A9.54ES
80.
60.
40.
20.
0.
22 > 00
0.0X0
line
-2.6X6
.2.1X6
.1.5X6
.1.0X6
.5.1X5
17:00 18,00 15(00 20.00 31.00
r±le:P973S48 tl-755 Acqil2-SXP-1997 15:06,10 SI+ Volttgm SIX 70P
375.8364 ExpiDB335
TRIANGLE LABS TmxttTLI M23 BLANK TLI443057R1
1001 .
22 tOO
0.0X0
Tin*
17.00
18.00
19,00
20100
31,00
22iOO
59
-------
*iJ.esFy/JU4U f 1-755 Acyili-SEP-1997 15,06llO XI+ Volt*ff* SIS 7OF NOLmmt483
319.8965 BSUS(256,30,-3.0y PXO(5,3,1,0.10\,1932.0,0.OQ\,r,T) X3CptDB225
TRIANGLE LABS TmXtlXLI H23 BIJOU TLII43 057X1
100* A3.251H
80.
IBiOO 19,00 30,00 21,00
rll*tP973848 #1-755 Aeq 112-SXP-1997 15,06,10 X1+ Voltag* SIX 7OP Hoi**,444
321.8936 BSOB(2S6,30,-3.0) PKD(5,3,1,0.10\,1776 .0,0.00\,f,r) Xxp,DB235
ZSXAHGXJC LABS ItorttXCX H23 3LAHK TLH430S7X1
1009k A3.98X4
22100
10100 19,00 20,00 21,00
rilf,P973B4a #1-755 Acgtl2-SXP-1997 15,06,10 XI+ Voltmy* SIX 7OP Bairn*,539
327.8847 BSO*(256,30,-3.0) PB>(5,3,1,0.10*,2156.0,0.00\,r,r) Xxp,DS225
TRIANGLE LABS TvcttXLX H23 BUOOi TLH43057*1
1001 A1.J.5X7
80.
60.
40.
20.
22,00
18,00 19tOO 20,00 21,00
ril»,P973848 #1-755 Acq,12-SXP-1997 15,06,10 XT+ Voltaym SIX 7OP Jfoi.au,903
331.9368 BSOB(256,30,-3.0) PKD(5,3,1,0.10\,3612.0,0.00\,r,T) Exp,DB225
TBIAWGXJT LABS T«Xt.-IXJ H23 BLANK XLH43057X1
1001 A7.45X6
22,00
80.
60.
40.
20.
AS.OSEi
18*00 19i00 20,00 21,00
rila,P973B4S #1-755 Acq,12-SEP-1997 15,06,10 XI* Voltagw SIB 70P Haifa,485
333.9338 BSOB(256,30, -3.0) PXJ>(5,3,1, 0.10\,1940.0,0.00\,T,T) Xxp,DB225
TRIAtKLX LASS TextiTLI M23 BLANK TLH43057X1
100$ A9.24X6
22,00
80.
60.
40.
20.
0.
A7.65.
.3.0X6
.2.4X6
.1.8X6
'.1.2X6
.6.1X5
0.0X0
Tim*
-2.0X6
.1.6X6
'.1.2X6
'.7.9X5
.4.0X5
.0.0X0
Tim:
,2.4X6
.1.9X6
.1.4X6
J.7X5
'.4.8X5
18 tOO
19*00
20100
211 CO
22100
.0.0X0
Tim<
mmm
-------
rilesP973848 #1-755 Aoq,12-SXP-1997 15t06ilO EI+ Voltagm SIS. 7 OP
303.9016 Xfp,DS225
TKIAMLX LABS r«xt»raj H23 SLABX zxrMJ057si
JOO]
17100 18:00 1*100 JOiOO Zl»00
rilt,P973848 fl-755 Aog,l2-BXP-1997 ISiOStlO XH- Volt*y* SIX 7OP
315.9419 XfpiDSSaS
TRIANGLE LASS TfXtiTLI H23 BLAST TLH43057X1
so:
40:
20:
17 17 19,23 30tSO 32,17 1
^AUvul^K
-.4
la
.0
22: 00
1001
so:
10:
20:
20,40
17,00 18,00 19,00 20,00 21,00
rilf,P973848 91-755 Acq,12-SXP-1997 15,06,10 XI+ Voltage SIX 70P
319.8965 Ecp,DB225
TXIANGLX LASS TazttZLJ H23 SLANT TLIt430S7Xl
22,00
1X4
.1X3
8X3
,5X3
,3X3
,0X0
Timt
,9X6
,6X6
,2X6
,8X5
.9X5
.0X0
Timt
17,00 18,00 19,00 20,00 21,00
ril»tP973848 tl-755 Aoy,12-SXP-1997 15,06,10 XX+ Vo£tagw SIS 70P
331.9368 ExpiDS325
TXIAXGLX LASS ToxttTLI M23 JUUOT TLIt43057Rl
lOOi
80:
sol
401
201
0.
22,00
,0X6
.6X6
.2X6
.0X5
.0X5
.0X0
17,00 18,00 19,00 20,00 21,00 23,00
rU.f,P973848 il-755 Acq,l2-SXP-1997 15,06,10 X1+ Voltage SIX 70P
292.9825 Xxp,DB22S
TSIASSLX LASS T*Xt:TLI M23 SLAKX TLIHJ057S1
18,58 19:46 20:16 30,44 31,33 22,00
1001
so:
60:
40:
20:
o.
16,55
17,46 18,22
.9X6
.3X6
.7X6
.2X6
.6X6
.0X0
17,00 18,00 19,00
rll»,P973848 fl-755 Aoq,12-SXP-1997 15,06,10
330.9793 Erp,DS235
TSIAIKLJC LASS TtoctiXLI H23 SLASX TLI«43057Xl
18,44 19,16
1003
aoj
601
40:
20:
ol
16,59
20,00 21,00
Voltmg* SIX 70P
19,52
22,00
22j46 8
.6
.5
.3
.1
1.0
.7X6
.9X6
.2X6
.5X6
.7X6
.0X0
17tOO
18100
19,00
30,00
31,00
33,00
-------
Ref, lass 292,9825 Peak top
Height 1,18 volts Span £88ppi
fl 292.9825
B 383,9816
C 385,8987
D 315,9419
E 317,9389
F 319,8965
6 321,8936
H 327,8847
I 338.9792
Systea file naae
Data file naie
Resolution
Group nuiber
lonlzatlon Mde
Mching
lasses 292,9825, 388,9761
1
El*
j 338,9792
K 331,9368
H 375,8364
Channel I 338,9792 Peak top
Heloht 1,15 volts Span 206 ppi
o
-------
TLI Project:
Client Sample:
43057rl
O-M23-4
Method 23 PCDD/PCDF Analysis (a)
Analysis File: S975865
Client Project:
Sample Matrix:
TLI ID:
Sample Size:
Dry Weight:
GC Column:
ASPHALT TtfWfT "ft
M23TRAIN
181-27-6A-C
1.000
n/a
DB-5
/
Date Received:
Date Extracted:
Date Analyzed:
Dilution Factor:
Blank File:
Analyst:
08/29/97
09/06/97
09/13/97
n/a
S975864
ML
Spike File:
ICal:
ConCal:
% Moisture:
% Lipid:
% Solids:
SPX23704
SF56117
S975861
n/a
n/a
n/a
Anaiyte* * / *"-% , ;
2,3,7,8-TCDD
1,2,3,7,8-PeCDD
1,2,3,4,7,8-HxCDD
1,2,3,6,7,8-HxCDD
1,2,3,7,8,9-HxCDD
1,2,3,4,6,7,8-HpCDD
1,2,3,4,6,7,8,9-OCDD
*mta*$:f
ND
ND
ND
0.01
ND
EMPC
0.09
^-T&^W^^"'-
0.004
0.005
0.006
0.005
0.04
>4:'^» x-?^?r;, ?to&
1.27 30:00
B_
0.93 35:22 B_
2,3,7,8-TCDF
1,2,3,7,8-PeCDF
2,3,4,7,8-PeCDF
1,2,3,4,7,8-HxCDF
1,2,3,6,7,8-HxCDF
2,3,4,6,7,8-HxCDF
U,3,7,8,9-HxCDF
1,2,3,4,6,7,8-HpCDF
1,2,3,4,7,8,9-HpCDF
1,2,3,4,6,7,8,9-OCDF
_ . .
totals „
Total TCDD
Total PeCDD
Total HxCDD
Total HpCDD
Total TCDF
Total PeCDF
Total HxCDF
Total HpCDF
0.02
ND
EMPC
0.03
0.01
0.02
ND
0.05
0.02
0.05
' Atnf fiirtV-1 *'
Aim, law 'i.
EMPC
0.01
0.07
EMPC
0.03
0.01
0.09
0.09
0.003
0.004
1 ffttmhnr f**
? fnaaocff IA>
1
3
3
1
5
3
0.01
. cworv •• •• ••
cmr?y
0.007
0.02
0.07
0.02
0.10
0.10
0.85
1.25
1.33
1.24
0.99
1.05
1.00
f V -,\
•• s
21:39
29:12
29:19
29:48
31:58
33:09
35:29
' •• s
"•% *" "• ^
B_
B
B_
B_
B^
iZ
B_
B_
x eta—
riags
—
Page 1 of 2
X237_PSR 12.00. LARS 6.IO.M
Triangle Laboratories, Inc.®
801 Capitola Drive • Durham, North Carolina 27713
Phone: (919) 544-5729 • Fax: (919) 544-5491
Printed: 17:51 09/14/97,
63
-------
TLI Project: 43057rl
Client Sample: O-M23-4
Method 23 PCDD/PCDF Analysis (a)
Analysis File: S975865
internal Standard*
IJC,2-2,3,7,8-TCDF
13O-2,3,7,8-TCDD
13C,2-l,2,3,7,8-PeCDF
13C,3-l,2,3J,8-PeCDD
13C,2-l,2,3,6,7,8-HxCDF
13C,2-l,2,3,6,7,8-HxCDD
13Cp-l,2,3,4,6,7,8-HpCDF
'3C,2-l,2,3,4,6,7,8-HpCDD
13C12-1,2,3,4,6,7,8,9-OCDD
Surrogate Standards {type A)
37Cl4-2,3J,8-TCDD
l3C,2-2,3,4,7,8-PeCDF
13C,2-l,2,3,4,7,8-HxCDF
13C,2-l,2,3,4,7,8-HxCDD
'3C,2-l,2,3,4,7,8,9-HpCDF
AJtemate Standards (Type A) ,
I3C,2-l,2,3,7,8,9-HxCDF
l3C,2-2,3,4,6,7,8-HxCDF
Recovery Standards
13C.2-1,2,3,4-TCDD
13Ci2-l,2,3,7,8,9-HxCDD
Amt, (jag)' V
4.8
3.9
4.3
4.5
4.5
4.1
3.5
3.6
5.5
Amt. (og)
4.3
3.7
3.9
3.4
3.9
Amt (119), ::-;
4.7
4.3
/'%R«SBV»rjj
120
98.7
107
112
113
103
88.5
90.1
68.8
^ /Of faSOQvta*
106
93.4
97.6
85.9
98.7
;V*w:J£R«t«l
117
107
- ' " ^\% "-'-•
^'QCtM^^
40%-130%
40%-130%
40%-130%
40%-130%
40%-130%
40%-130%
25%-130%
25%-130%
25%-130%
jfv ^uMr
70%-140%
70%-140%
70%-140%
70%-140%
70%-140%
y:wQG Limits
*<**:.$ -,f < -f
40%-130%
40%-130%
„ -, ,\ "- -;,
^^rtte^;
0.76
0.79
1.46
1.55
0.51
1.24
0.42
1.03
0.92
IX Bfc^^
1.44
0.50
1.26
0.42
>%X1UU&$&
0.51
0.51
S ?"• : •*•. f*-- \t ,
0.81
1.24
BT Flags-
21:37
22:23
25:41
26:45
29:18
29:59
31:57
32:48
35:22
"5 fnr ^ ^lags
22:23
26:24
29:12
29:55
33:08
%x.£ Hl*Ajf* *^ 5i Plflfl®'
30:29
29:47
^RT.\ ?**&*
22:11
30:17
Data Reviewer.
-10
Page 2 of 2
09/14/97
X237 _PSR »10a LARS 6.10.04
Triangle Laboratories, lnc.»
801 Capitola Drive • Durham, North Carolina 27713
Phone: (919) 544-5729 • Fax: (919) 544-5491
Printed: 17:51 09/14/97
64
-------
Initial
. .Date...
)ata Review By:
Calculated Noise Area: 2.22
'he Total Area rcr each peak with an ion abundance ratio outside
ratio limits has been recalculated according to method requirements.
>age No.
39/14/97
Listing of S975865B.dbf
Matched GC Peaks / Ratio
/ Ret. Time
:ornpound/
d_Z.... QC.Log Omit Why . .RT. OK Ratio Total.Area. .. Area.Peak.1. . Area. Peak. 2.. Rel.RT Cocnpound.Name. .
ID.. Flags.
TCDF
504-306
304-306
D
D
A
DC
DC
DC
DC
d
DC
d
DC
NL
SN
SN
SN
SN
SN
SN
SN
3
0:
18:
13:
20:
20:
21:
21:
21:
00
18
35
33
53
12
28
39
22:04
22:
23:
22
22
0.
RO
RO
RO
RO
RO
RO
RO
65-0.89
1
0
0
0
1
0
0
0
1
0
0
.00
.54
.67
.55
.13
.84
.52
.85
.05
.37
.66
Peaks
0
3
1
5
7
28
3
39
6
1
13
81
.23
.65
.84
.33
.24
.09
.72
.70
.05
.95
.66
.45
0.838-1.092
0.000
0.847
0.860
0.951
12.84
18.25
0.
15.25 0.
0.
21.45 1.
1.
1.
.966
981
.993
.002
.021
,035
2378-TCDF
5.45
AN
8.21 1.081
13C12-TCDF
316-318
316-318
0.65-0.89
DC NL 0:00 RO 0.39
0.954-1.046
0.34
21:11
21:37
22:05
3 Peaks
0.72
0.76
0.76
«h
34.00
7,668.11
29.48
7,731.59
ova- TCHP / TV
14.26
3,317.31
12.75
19.74 0.980
4,350.80 1.000
16.73 1.022
0.000
0.980
1.000 13C12-2378-TCDF ISO
TCDD
320-322
320-322
DC
DC
d
DC
DC
d
DC
DC
DC
DC
DC
d
DC
DC
DC
DC
DC
NL
HL
SN
SN
SN
SN
SN
SN
SN
SN
SN
SN
SN
SN
SN
SN
SN
1
0
19
19
:00
:31
:45
20:15
20
20
21
21
21
21
21
22
22
22
22
22
23
23
:25
:54
:10
:22
-.29
:37
:49
:04
:17
:36
:41
:49
:03
:15
0.
RO
RO
RO
RO
RO
RO
RO
RO
RO
RO
RO
RO
RO
RO
RO
65-0.89
2
1
1
0
1
0
0
0
1
2
0
2
0
1
0
0
0
1
.21
.26
.04
.60
.41
.41
.83
.76
.35
.09
.59
.35
.91
.38
.38
.67
.13
.10
Peak
0
1
10
6
2
0
6
2
1
2
2
0
5
1
0
1
0
2
10
.34
.03
.34
.53
.60
.69
.92
.32
.49
.07
.34
.60
.42
.03
.71
.05
.46
.23
.34
6.08
0.875-1.055
0.000
0.872
5.84 0.882
0.905
0.912
0.934
0.946
0.955
0.960
0.966
0.975
0.986
0.996
1.010
1.013
1.019
1.030
1.039
Triangle Laboratories, Inc.® Analytical Services Division
301 Caprtola Drive • Durham, North Carolina 27713
3hone: (919) 544-5729 • Fax: (919) 544-5491
Printed: 17:51 09/14/97-
-------
Page No.
09/14 97
Listing of S975865B.dbf
Matched GC Peaks / Ratio / Ret. Time
Compound/
M_2.... QC.Log Omit Why ..?.T. OK Ratio Total .Area... Area. Peak. 1. . Area. Peak. 2. . Rei.RT Compound. Name. . ID.. Flags.
37C1-TCDD
323
328
13C12-TCDD
332-334
332-334
PeCDF
340-342
H
340-342
13C12-PeCDF
352-354
DC NL 0:00
2Z.23
1 Peak
DC NL 0:
21:
22:
22:
22:
00
09
11
23
43
0.
RO
RO
4
4
0.
.561.
,561.
47
50 4,561.50
50
65-0.89
4.
1.
0.
0.
0.
4 Peaks
DC NL 0:00
DC SN 23:
DC SN 23:
DC SN 24:
DC SN 24:
24:
DC SN 25:
DC SN 25:
DC SN 25:
DC SN 25:
DC SN 26:
26:
DC SN 26:
DC SN 27;
DC SN 27:
DC WH 27:
40
57
35
42
47
09
24
50
58
09
25
50
04
31
47
1.
RO
RO
RO
RO
RO
RO
RO
RO
RO
RO
RO
RO
RO
RO
09
08
81 4
79 5
86
10
32-1.78
1.
2.
0.
0.
1.
1.
1.
5.
2.
2.
3.
1.
1.
3.
0.
0.
03
79
66
97
23
52
57
98
23
09
57
83
02
06
77
39
2 Peaks
DC NL 0:
24:
00
49
25:18
25:
25:
25:
41
50
58
1.
RO
RO
0.
20.
,829.
,081.
75.
,007.
57
87 12.71
18 2,166.73
62 2,248.91
34 34.92
01
0.910-
c* .
1.090
000
000 37C1-7C3D
SUR1
0.910-1.090
11.79
2,662.45
2,832.71
40.42
0.
0.
0.
1.
1.
000
945
991 13C12-1234-TCDD
000 13C12-2378-TCDD
015
RSI
IS1
TC DD / P0C DP Fo 1 1 ows
0.
5.
1.
1.
4.
15.
6.
4.
3.
5.
1.
17.
4.
1.
1.
0.
32.
61
94
37
88
01
41 9.30
31
13
80
92
17
01 12.20
08
73
30
71
42
,32-1.78
1.
1.
00
60
1.90
1.46 5
26:24
27:22
352-354
PeCDD
356-358
RO
1.
1.
1.
54
53
44 5
1.02
7 Peaks
DC NL 0:00
DC WL 24:
24:
:44
• 56
DC SN 25:15
1
RO
RO
RO
RO
11
.32-1.78
0.83
6.00
1.28
2.84
0.
21.
25.
,880.
20.
32.
23
77 13.39
09 18.71
80 3.488.97
34 12.33
07 19.38
,329.39 3.141.80
11.86 7.21
0.915-1.074
6.11
6.67
0.
0.
0.
0.
0.
0.
0.
0.
1.
1.
I.
1.
1.
1.
000
921
933
957
962
965
979
989
006
Oil
018
029 23478-PeCDF
045
054
AN
1.071
1.082
0.
844-1.156
0.000
8.38
9.84
2.391.83
8.01
12.69
2.187.59
7.08
0.966
0.985
1.000 13C 12 -PeCDF 123
IS2
1.006
1.
1.
,011
.028 13C12-PeCDF 234
SDR2
1.066
,321.32
PcCPP / P<*tDD Pel 3. ows
0.
0.16
0.31
7.86 4.78
926-1.024
0.000
0.
.925
3.74 0.932
0.48
0.944
Triangle Laboratories, Inc.® Analytical Services Division
801 Capftola Drive • Durham, North Carolina 27713
Phone: (919) 544-5729 • Fax: (919) 544-5491
Printed: 17:51 09/14/1
-------
Page No.
39 '14/97
Compound,
Listing of S975865B.dbf
Matched GC Peaks / Ratio / Ret. Time
QC.Log Omit Why ..RT. OK Ratio Total.Area.., Area.Peak. 1.. Area.Peak.2.. Rel.RT Compound.Name.. ID.. Flags.
K
356-358
13C12-PeCDD
368-370
368-370
HxCDF
374-376
D
D
374-376
13C12-HXCDF
384-386
N
384-386
DC SN
DC SN
DC SN
DC SN
DC SN
DC SN
DC WH
3
DC NL
DC SN
2
DC NL
d SN
DC SN
DC SN
DC SN
d SN
DC SN
DC SN
DC SN
DC SN
6
DC NL
DC SN
5
25:30
25:41
25:59
26:28
26:36
26:46
26:54
27:07
27:30
Peaks
0:00
26:28
26:45
26:54
Peaks
0:00
28:14
28:22
28:39
28:49
28:59
29:12
29:19
29:25
29:36
29:48
29:56
30:08
30:31
30:34
30:37
Peaks
0:00
28:21
29:12
29:18
29:34
29:47
30:29
Peaks
RO
RO
RO
RO
RO
RO
RO
RO
1.
RO
RO
1.
RO
RO
RO
RO
RO
RO
RO
RO
RO
RO
0
RO
RO
0.87
1.71
1.94
4.73
0.48
2.18
2.68
1.02
0.75
32-
0.
1.
1.
1.
1.78
83
27
55 3,
55
3.
ftV.A*» . 1
0.76
12.35 7.80
5.89 4.47
2.04
1.10
3.19
1.12
0.89
1.05
26.10
0.953
4.55 0.960
2.31 0.971
0.989
0.994
1.001 12378-PBCDD
1.006
1.014
1.028
AN
0.850-1.150
0.
3.
437.
274.
711.
»**/-T\n
05-1.43
1.
1.
1.
0.
0.
5.
1.
1.
1.
1.
1.
2.
0.
0.
1.
0.
21
21
34
95
77
85
25
33
81
44
24
02
24
77
01
79
2.
15.
35.
6.
4.
0.
50.
23.
4.
10.
28.
1.
0.
3.
9.
1.
162.
16
06
52 2,090.64
11 166.48
63
54
56 8.51
02 20.04
02
21
45
54 28.07
99 13.68
88
12
71 15.88
10
51
97
10 5.04
45
92
.43-0.59
1.
0.
0.
0.
0.
0.
0.
00
56
50 4
51 5
.26
.51 4
.51 4
19
2.49
8.55 3.07
,955.
.40 1,656.35
,294.90 1,782.26
2.58
,637.
.69 1,563.79
,428.48 1,493.87
0.
0.
1,346.88 1.
107.63 1.
000
989
000 13C12-PeCDD 123
006
IS3
0.959-1.050
0.
7.05 0.
14.98 0.
0.
0.
0.
22.47 0.
000
964
968
978
984
989
997 123478-HXCDF
10.31 1.001 123678-HXCDF
1.
004
AN
AN
1.010
12.83 1.017 234678-HxCDF
AN
1.022
1.028
1.042 123789-HXCDF
AN
4.97 1.043
1.045
0.863-1.137
0.000
5.48 0.968
3,299.05 0
.997 13C12-HXCDF 478
3,512.64 1.000 13C12-HXCDF 678
SUR3
1S4
1.009
3.073.90 1
.016 13C12-HXCDF 234
2,934.61 1.040 13C12-HXCDF 789
ALT2
ALT1
.325.02
Above: HxCDF / HxCDD Follows
Triangle Laboratories, Inc.® Analytical Services Division
801 Caprtola Drive • Durham. North Carolina 27713
Phone: (919) 544-5729 • Fax: (919) 544-5491
Printed: 17:51 09/14/97—
u7
-------
?>ge No. 4
C9 14/97
Compound/
!•!_: .... QC. Log Omi t Why
Listing of S975865B.dbf
Matched GC Peaks / Katie
/ R*t. Tirae
.RT. OK Ratio Total.Area... Area.Peak.1.. Area.Peak.2.. Rel.RT Corapound.Name.. ID.. Flags.
KxCDD
330-392
D
390-392
13C12-HXCDD
402-404
402-404
HpCDF
408-410
H
408-410
13C12-HpCDF
418-420
418-420
DC NL 0:00
DC SN ;8:45
DC SN :8:50
DC SN 39:00
29:12
DC SN 29:17
DC SN 29:56
30:00
d SN 30:17
DC WH 30:30
DC WH 30:38
3 Peaks
1.05-1.43
RO 0.90
RO 0.66
RO 0.27
RO 5.35
1.30
RO 1.76
1.27
RO 0
1
1
RO 1
RO 0
.59
.27
.18
.01
.42
1
4
0
0
41
3
20
3
12
10
2
0
75
.79
.50
.38
.83
.69
.09
.79
.50
.73
.77
.01
.54
.21
23.
11.
7.
54
63
11
1.05-1.43
DC NL 0.: 00
29:24
29:55
29:59
30:17
4 Peaks
1
1
1
1
1
.08
.10
.26 3
.24 3
.24 3
11
3
14
,341
.998
,896
,251
UwOTY
.28
.96
.80
.61
.41
.78
rt /
0.88-1.20
DC NL 0:00
31:58
32:11
32:18
DC SN 32:51
33:09
DC WH 33:20
4 Peaks
RO 1
0
RO 1
0
RO 0
1
RO 0
.56
.99
.42
.92
.69
.05
.26
4
57
13
18
3
19
3
109
.08
.69
.73
.53
.96
.72
.24
.67
7.
1,862.
2,212.
2,157.
82
50
03
96
0.953-1.014
0.000
0.959
0.962
0.967
18.15 0.974
0.977
9.16 0.981
5.62
0.
1.
1.
1.
1.
998 123478-HXCDD
001 123678-HXCDD
010 123789-HxCDD
017
022
AN
AN
AN
0.967-1.033
7.14
1,479.30
1,786.58
1,738.45
0.
0.
0.
1.
1.
000
981
998 13C12-HXCDD 478
000 13C12-HXCDD 678
010, 13C12-HXCDD 789
SUR4
IS5
RS2
28.
9.
8.
10.
69
55
88
10
0.37-0.51
DC NL 0:00
31:57
32:30
32:46
33:08
33:20
5 Peaks
RO 1
0
RO 0
RO 2
0
RO 0
.39
.42 3
.25
.72
.42 2
.18
5
3
,058
14
6
,327
68
,476
Hrrf-n
.12
.65
.27
.84
.94
.69
.39
p /
906.
4.
12.
685.
20.
Hnf-nn Poll^
47
36
91
97
99
0.
29.00
6.73
9.65
9.62
0.
2,152.18
17.37
4.75
1,641.97
118.75
995-1.042
0.
1.
1.
1.
1.
1.
1.
000
001 1234678-HpCDF
007
Oil
028
038 1234789-HpCDF
043
AM
AN
937-1.125
0.
1.
1.
1.
1.
1.
000
000 13C12-HpCDF 678
017
026
037 13C12-HpCDF 789
043
IS6
SOR5
HpCDD 0.88-1.20
424-426 DC NL 0:00 RO 2.13 4.22
M 32:12 RO 1.54 19.26
M 32:48 RO 1.23 32.44
DC WH 32:59 RO 6.14 5.20
DC WH 33:14 RO 5.99 4.32
14.50
19.60
0.977-1.005
0.000
9.44 0.982
15.90 1.000 1234678-HpCDD
1.006
1.013
AN
Triangle Laboratories, Inc.® Analytical Services Division
801 Caprtola Drive • Durham, North Carolina 27713
Phone: (919) 544-5729 • Fax: (919) 544-5491
Printed: 17:51 09/14/J
-------
Page Mo.
09/14/97
Listing of S97«53B.dbf
Hatched GC Peaks Ratio / Ret. Time
Compound/
M_Z.... QC.Log Omit Why ..RT. OK Ratio Total.Area... Area.Peak.1.. Area.Peak.2. . Rel.RT Compound.Name.. ID.. Flags.
424-426
2 Peaks
51.70
13C12-HpCDD 0.88-1.20 0.969-1.031
436-438 DC NL 0:00 1.13 1.51 0.000
32:12 RO 0.77 5.77 2.94 3.83 0.982
32:48 1.03 2.861.43 1,452.51 1.408.92 1.000 13C12-HpCDD 678 1ST
436-433 2 Peaks 2.867.20
OCDF
442-444
442-444
OCDD
458-460
458-460
13C12-OCDD
470-472
470-472
DC
DC
DC
DC
DC
DC
DC
DC
DC
DC
DC
DC
DC
DC
DC
DC
DC
NL
WL
SN
SN
SN
SN
SN
SN
SN
SN
SN
1
NL
SN
SN
SN
SN
1
NL
1
0
31
31
31
32
32
33
33
34
35
35
35
:00
:20
:40
:54
:27
:40
:29
:59
:41
:29
:39
:52
0.
RO
RO
RO
RO
RO
RO
RO
RO
RO
76-1.02
0
0
0
0
0
0
2
0
0
1
1
0
.60
.38
.33
.11
.37
.51
.28
.69
.96
.00
.18
.91
Peak
0
35
35
35
35
35
:00
:09
:22
:34
:41
:47
0.
RO
RO
RO
RO
76-1.02
1
0
0
3
0
1
.25
.95
.93
.30
.44
.09
Peak
0
35
:00
:22
0.
RO
76-1.02
1
0
.20
.92
Peak
Above: »pCBD / Octa-CDD and CDF Follows
0.74
0.85
0.62
0.32
0.62
0.89
0.76
0.66
.80
1.
23.40
1.74
1.62
23.40
0.30
1.07
33.80
0.43
0.51
1.66
33.80
0.19
2,782.87
2,782.87
11.70
0.887-
0.
0.
0.
0.
0.
0.
0.
0.
0.
11.70 1.
1.
1.1]
000
886
895
902
918
924
947
961
981
003
008
L3
OCDF
16.30
1.014
0.887-1.113
0.000
0.994
17.50 1.000 OCDD
AN
006
009
1,335.35
1.012
0.996-1.005
O.OOO
1,447.52 1.000 13C12-CCDD
IS8
Column Description "Why" Code Description QC Log Desc.
M_Z -Nominal Ion Mass(es)
..RT. -Retention Time (mm:ss)
Rat.l -Ratio of M/M+2 Ions
OK -RO=Ratio Outside Limits
Rel.RT-Relative Retention Time
End of Report
WL-Below Retention Tine Window
WH-Above Retention Time Window
SN-Below Signal to Hois* Level
-------
'il«iS975865 tl-905 Acq,13-SXP-1997 00,54,19 Ell- Voltfgm SIX 70S Holt*,65
303.9016 r,2 BSOB(256r30,-3.0) PKD(9,5,5,0.05\,360.0,1.00\,r,T) XzpiXTCUS
TRIANGLE LABS Tert:O-M2J-4 TLH43057K1 X1K7. TIMS • 00.57
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80:
60:
40:
20:
19.00 20*00 21.00 22*00
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305.8987 tt2 BSUB(256,30,-3.0) tXD(9,S,5,0.05\,268.0,1.00\,r,T) XxptXPCUS
TXIAVBLE LABS TartiO-M23-4 TLIt43057Xl BKT. TIME - 00.57
1001 A2.J.4E5
19,00 20*00 21*00 22.00
HZ*.S975865 tl-905 Aoqtl3-SXP-1997 00.54.19 XI+ Voltage SIX 70S Soim»t76
315.9419 rs2 BSUB(256,30,-3.0) tXD(9,S,5,O.OS\t304.0,1.00\,T,T) XrptXPCtJS
TRIANGLE LABS Text.O-M2.3-4 TLH43057R1 ZKJ. TIME - 00.57
1001 A3.32X7
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50:
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20:
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317.9389 JPi2 BSVB(256,30,-3.0) tXD(9,5,5,0.05%, 75ff.0,1.00\,T,X) XrpiXPCOS
TXIASSLX LABS TaxtiO-M23-4 TLIt43057Xl IKT. TIME • 00.57
1001 A4.35X7
80:
50:
20:
20.00 21 * 00 22.00
rll»,S975865 tl-905 Aoqil3-SXf-1997 00,54,19 EH- Voltage SXJt 70S
330.9792 T:2 ExpiEPCUS
TRIANGLE LABS Z"ezt.O-M23-4 IXT#43057£1 XK7. TZMK - 00.57
23tOO
19*00 20*00 21*00 22*00
rll»,S975865 tl-905 Acqil3-SXT-1997 00*54.19 n* Voltage SIX 70S
375.8364 F*2 XxpiXPCOS
TXIASSLX LABS T«ztx0-M23-4 ZEJM3057J11 UCT. 37MK • 00*57
23,00
100J
80:
60.
40:
20:
0:
18
183°
34
19*31
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19*07
I 21*14
JwwLAjuL^s««JLv>,
21i42
.14*00
20>00
21.00
'22.00
23'iOO
-4.2C4
.3.3E4
'.2.5X4
'.1. 7X4
'.8.3X3
-.0.0X0
Time
5.7X4
.4.6X4
'•.3.4X4
.2.3X4
.1.1X4
0.0X0
HM*
.9.8X6
17.9X6
Is.9X6
.3.9X6
.2.0X6
0.0X0
-1.3X7
.1.0X7
.7.7X6
J.1X6
.2.6X6
0.0X0
.9X3
70
-------
FiletS97S865 il-905 Acqtl3-SEP-1997 00i54il9 £1+ VoltMgm SIX 70S Nairn*t208
319.8965 r,2 BSUB(256,30,-3.0) PKD(7,5,3,0.05\,832.0,1.00\,r,T) XxptEPCOS
TRIANGLE LABS Text:O-M23-4 TLH43057X1 IKT. TIMS ' 00:57
ion
eo:
20100 31:00 22:00 23:00
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321.8936 Ft2 BSUB(256,30,-3.0) PKD(7,5,3,0 .OS\,384.0,1.00\,T,T) XxpiXPCUS
TRIANGLE LABS T*zt:O-M23-4 TLH43057X1 OKT. TIME • 00:57
1001
801
20:00 21>00 22:00 23,00
fil»:S975865 il-905 Acq,13-SXP-1997 00,54,19 EI+ VoltJtg* SIX 70S Hoifm,655
331.9368 T,2 BSUB(256,30,-3.0) PlO>(7,5t3,0.05\,2620.0f1.00\,T,T) ExptEPCOS
TRIANGLE LABS Taxt:O-H23-4 TLH43057X1 HC7. TIKE - 00i57
1001 A2.J.7X7
80:
40:
20:
20100 21s00 22:00 23:00
rll»iS975865 il-905 Aoqil3-SEP-1997 00:54:19 fH- Voltmg* SIX 70S Soif»:162
333.9338 Tt2 BSUB(256,30,-3.0) PKD(7r5,3,0.05\,648.0,1.00\,f,T) SzptXPCUS
TXXASGLE LABS T*zt.:O-M23-4 XLH43057X1 JXT. TIME - 00:57
100* A2.66E7
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60:
40:
20:
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20100 21100 22100 23:00
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327.8847 T:2 BSUB(256,30,-3.0) PXS(7,5,3,0.051,940.0,1.00\,r,T) ExptSPCUS
TRIANGLE LABS TexttO-M23-4 TLH43057S1 IKT. TIKE " 00:57
1003
80.
60:
40:
20:
0.
20,00 21,00 22,00
Pllm:S975865 il-905 Acq,13-SXP-1997 00,54,19 Ell- Vdltmym SIX 70S
330.9792 f,2 XxptEPCOS
TXIASSLX LABS T*ztiO-M23-4 TLH43057X1 HOT. TIME
23:00
00,57
52 23,07
.6.2X6
.5.0X6
.3.7X6
.2.5X6
-.1.2X6
.0.0X0
TimtA
-7.7X6
'•.6.2X6
.4.6X6
-.3.1X6
.1.5X6
0.0X0
-.1.2X7
-.9.9X6
:.7.4X6
.5.0X6
.2.5X6
.0.0X0
20,00
21,00
22,00
23:00
71
-------
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339.8597 r,2 3503(356,30,-3.0) PXD(7,5,3, 0.05%, 748.0,1.00\,r,T) XxptXPCOS
TXIAOSLX LABS T«Xt>O-M23-4 TLH43057S1 XK7. TDtK - 00.57
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24.00 35100 26 > 00
Til»tS975865 tl-905 Acq,13-8XP-1997 00.54.15 EI+ Voltag» SIM 70S Ooimmtiai
341.8567 F>2 BSO3(356,30, -3.0) PKD(7,5,3,0.05%, 724.0,1.00%,JT,T) XxpiXPCOS
LABS Z>*rt>0-M23-4 IXT*43057JU Off. XXMf - 00,57
27100
34 tOO 25tOO 26 tOO
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351.9000 Tt2 BSVS(356,30,-3.0) PXD(7,5,3,0.051,284.0,1.00\,r,T) XxptXPCOS
TXIANGLE LASS Tert:O-M23-4 TLH43057K1 OfT. TOOC - 00/57
37.00
100J
so:
20:
o:
A3.49*7
34,00 25,00 26,00 27,00
rilatS975865 tl-905 Acqtl3-SEP-1997 00i54tl9 XI* VoJtay* SIM 70S Holm*,70
353.8970 Tt3 SSO3(256,30,-3.0) PKD(7,5,3,O.OS\,280.0,1.00\,r,r) XrptXTCUS
LASS Text:0-N23-4 TLH43057K1 OCT. TOtg " 00,57
1001
ao:
60.
40:
20:
A3.39X7
A3.19X7
24,00 25,00 26tOO
TH*,S97S865 41-905 AcqtlS-SXP-1997 00,54,19 XH- Voltmgm SIM 70S
330.9792 r,2 XxptXPCOS
TMIAHGLX LABS Tert:O-M23-4 TUt43057Xl UKT. TIMX
60:
40:
20:
27,00
00,57
26,47 37,09
7,36.
34,00 35,00
ril»,S97586S tl-905 Acq,13-SXP-1997 00,54,19 tt+
409.7974 Tt2 XxptXfCOS
HGa LABS r«xt.O-*23-4 TUt43057Xl
1004
,23,36
80J 25,
60:
40:
20:
26,00
SIM 70S
27,00
ntr. TOIX - O0t57
27
25,54
26,36
06
24,00
25100
26,00
27,00
J.2E6
.6.9X6
.4.6X6
.2.3X6
0.0X0
XimtA
-8.1X6
.6.5X6
.4.8X6
.3.3X6
J..6X6
0.0X0
Ha.
,.9.4X6
7.5X6
.5.6X6
.3.8X6
.1.9X6
0.0X0
-7.SX3
.6.2X3
.4.7X3
.3.1X3
.1.6X3
-.0.0X0
72
-------
filaiS97Sa65 tl-905 AcqtlJ-SEP-1997 00,54,19 EI+ Vbjltage SIX 70S MaiftlSl
355.8546 Tt2 BSUB(256,30,-3.0) PXD(7rS,3,O.Q5\,204.0,1.00\,r,T) XxptXPCUS
TSIANSLX LABS TexttO-M23-4 TLH43057X1 XKT. TIMS - 00t57
1004
00:
eo:
40.
20.
g.
A7.80E4
fl A4.47E4
A4 . 78E4 1 1 II
A A2.73E4
\ A3. 78X4 kA1.i8E4
\ r-f°M ijii»s-«Wr f
J \A5.00E3 A4.56E3 1 \ KA I U A1.26E4h/\k A N\ K A8.84X3
24', 48 25>bb 25', 12 25 ',24 25\36 25', 4 8 26', 00 26*, 12 26\24 26'i36 26', 4 8 27', 00 27', 12 27:24 27', 36
-2.3E4
11 . 8E4
-1.4X4
-9.2E3
.4.6X3
'0.0X0
Tile,S97586S tl-905 Aoqtl3-SXP-1997 00,54,19 EH- Voltage SIX 70S Soif»i58
357.8516 Fi2 BSUB(256, 30, -3.0) PKD(7,5,3,0.05\,232.0,1.00\,r,T) XxptXPCUS
TXIA1KLX LABS T*XtsO-M23-4 TLI«43057X1 HKT. TIME - 00i57
1003
00:
so:
40.
20.
A4.55X4
A3.74E4
J 1 A2.31E4 A1.39X4
M A 1
flf 11 \ •"•'•f*^.. ,» A1.2SE4
II /\ \ , (A7'?9X3R i I ,» , A8.50X3
1 \ M p* fj*S. 26X31 \ , \ A "Jl A A All WMI-39X3A5-30X3 j, 7J1j A
24\48 25tbb 2S\12 25t24 25\36 2s', 4 8 26', 00 26ti'2 26', 24 26', 3 6 26t48 27', 00 27', 12 27', 24 27', 36
-2.1X4
'.1.7X4
'.1.3X4
'.0.5X3
'.4.3X3
T±»m
Til»iS975865 tl-905 Aesqtl3-SXP-1997 00*54,19 XH- Voltag* SIX 70S *>!*•> 50
367.8949 T,2 BSOB(256, 30, -3.0) PJKD( 7,5,3, O.OS\,200.0,1.00\,r,T) XxptSPCOS
TXIANGLE LABS T*Xt,0-M23-4 TLH43057R1 HOT. TIMS - 00i57
1003
00:
60,
40.
20.
OJ
A2.09E7
\
\fl.66E6
J \ _/\
24', 4 8 '25,00 25', 12 25:24 25:36 25 ',4 8 26', 00 26', 12 26 ',2 4 26', 3 6 2 6 ',4 8 2?', 00 27', 12 27', 24 2?', 36
-7.4X6
'.5.9X6
'.4.4X6
'.3.9X6
'-1.5X6
0.0X0
Tim*
rilatS975865 tl-905 Aoq:13-SEP-1997 00,54,19 Eli- Voltage SIX 70S No±*a,61
369.8919 f:2 BSOB(256,30,-3.0) PXD( 7,5,3,0 ,OS\,244. 0,1. 00\,r,T) XxpiXPCUS
TRIAWSLX LABS Taxt:O-H23-4 TLIt43057Xl HKT. TIME - 00>57
1001
00:
60.
40.
20:
OJ
A1.35X7
1 Vu.oare
7 ry\
24I:48 25\b'o 2sVl2 25\24 25^36 25^48 26\00 26', 12 26', 24 26\36 26', 4 8 J7:00 27', 12 27', 24 27\36
-5.0X6
.4.0X6
'.3.0X6
.2. 0X6
.1.0X6
Tim*
rila,S975865 tl-905 Aoqtl3-SXP-1997 00,54,19 EH- Voltage SIX 70S
330.9792 r,2 XxptXPCUS
TXIANGLX LABS TuxHiO-H23-4 TLH43057X1 OUT. TIMS - 00.57
100]
00.
60.
40.
20:
o:
sA5l\A f\35'31 35r\° S\ 36l2*a6tlB 2*jf7 26'S*37'09 27,20
V
34\4»2S\Masli2'aiW23\3f'M^^
-9.4X6
.7.5X6
.5.6X6
.3.8X6
.1.9X6
0.0X0
Tim*
73
-------
F11«,S975865 fl-346 Acq t 13 -SEP -1997 00,54,19
XI + Volt*y» SIX 70S Hoif»:697
373.8208 T,3 BSOB(256,30,-3.0) PKD(7 , 5,3,0. 05\, 2768. 0,1. 00\,
TXIANGLX LABS TexttO-M23-4 TLH43057X1
1003
sol
SO:
40:
20.
A2.81X5
A2.00X5 |\
rt
"n\ .^v J\j
28,12 28124 iflijff 28 ,48 29:66 2 9': 12
ril»:S975B65 fl-346 Acq:13-BEP-1997 00,54,19
37X5
r,T) xxpiircas
UKT. TIMX m 00:57
-9.5X4
\ A1.59X5
\ A6.53X4 j[ AS. 04X4
V%/V/ Vsf£«L.. .. ^A-T -t- -A
.7.6X4
.5.7X4
.3.8X4
.1.9X4
-0.0X0
29:24 29:36 29:48 30,00 30:12 30,24 30,36 30,48 31*00 T±ma
XI+ Voltmgm SIX 70S Boi*»,573
375.8178 r,3 BSOB(256,30,-3.0) PKD(7,S,3,0.05\,2292.0,1.00\,r,T) XxpiXPCOS
TSIAKGLE LABS TfXt:O-H23-4 TLIf43057Xl
iota
80:
so:
40:
20:
JK7. ma - oot57
-1.9X3
A2.25X5
A1.50X5 h.
*7.05«A /\ ,
A J\ A3^P"^ . . J\J
38:12 28,24 28t36 28': 4 8 29t66 29,12
rilm,S975865 tl-346 Acq,13-SXP-1997 00,54,19
k A1.28X5 M 9?M
-.1.5X5
'.1.1X5
-.7.5X4
'.3.8X4
29: 34 29t36 29i48 JbioD jbiij 30\24 36:36 30148 3l',00 TLm*
XI+ Voltage SIS 70S Bolm»*823
383.8639 T:3 BSVB(256,30,-3.0) PKD(7,5, 3, 0.05%, 3292.0,1.00\,
XSIAXGLX LABS Tait:0-H23-4 TLH43057X1
1001
sol
sol
40:
20:
o:
I1
SB': 12 28': 24 '28,36 28,48 29,66 29,12
T,T) XxptXfCUS
XK7. ma - 00,57
A1.56X7 flt_.
I A1.49X7
\ _y_
ft
V J \
.6.8X6
.5.4X6
.4.1X6
.2.7X6
.1.4X6
'•o.oxo
29\24 29] 36 29:48 30:66 30:12 36:24 30,36 36:48 3l',6o TLmtt
rila:S975865 fl-346 Acq: 13 -SEP -19 97 00,54,19 XI+ Voltmgm SIX 70S Holm*, 823
385.8610 r,3 BSUB(256,30,-3.0) PKD(7,5,3,0 .05\, 3292.0,1.00\,T,T) XxpiXTCOS
TSIAHSZX LABS TaitiO-H23-4 ILH43057S1
1001
80:
so:
40:
20:
o-
A3. 30X7
I
I
y v
28': 12 28,24' '28:36' 28:48 29,00 29',12
A3.,
L J
HKT. ma • O0t57
^1.3X7
17X7
A3. 93X7
L y v
.1.1X7
.8.1X6
.5.4X6
.2.7X6
0.0X0
' 29':24' '29':36' 29':48"36':66 joiji' 3b',24' jbi jtf' J0»48 ' JiiOO Time
Tile:S975B65 fl-346 Aoq,13-SXf-1997 00,54,19 XI+ Voltage SIS 70S
392.9760 Fi3 XxpiXPCUS
TSIAXSLX LABS TextiO-M23-4 TLH43057S1
100*
80:
sol
401
30:
ol
2*>1° 28,20 28,37 *«i" ^9l°7
AAAA w^r\ « _^_ « ^r\*s\ r^ni\ . «.
^•--v- » ^^\/V *r~*\pf ' ^ ' VV"
28:12' 28't24' 28,36' 281, 4 8 "29', 66' 29', 12
"i" "s&^
A^Vvv^^
XK7. TIMX - 00,57
29,57 30:2130:31 tn,j<
/H /-JW/\A «A/W. «/WA— ..r »^C «/-^
i9,sfJ\\ fiT^ VUw^'W' »^^V/v^vV
/^"^ \y
u ^
.4.7X6
'•.3.8X6
.2.8X6
'•.1.9X6
-.9.4X5
'•o.oxo
' 291: 24' 29': 36' 29': 4 8 3t>',66 36:12 36:24 30: 36' 30', 48 3l'iOO T±M»
ril*:S975B65 fl-346 Acq,13-SXP-1997 00,54,19 EI+ VoltMf* SIS 70S
445.7555 Tt3 XxptXPCtJS
ttlABSLX LABS X»jrt,O-H23-4 TLH43057X1
lOOi
eol
SO.
40:
20.
0.
1
3O. tf
IKT. TDCT - 00»57
^.2.1X4
i ia,i*
m^^^j3i^^^^
28': 12 *28i24' iiljff' 28': 4 8 29:66 29': 12
' 29:24' 29': 36 29
.1.7X4
ll.3X4
.8.4X3
.4.2X3
'• o.oxo
i48 jotoo Jbiia jot24 jb
-------
rU.*lS975B65 tl-346 ActftJ.3-SEP-1997 OOlS4tl9 BI+ Valttf* SIS 70S Koif»,495
389.8156 Ti3 BSOB(256,30,-3.0) PXD(7,5,3,0.05\,1980.0,1.00\,r,T) XxptXPCOS
TRIANGLE LABS T*It>O-M23-4 TLIt43057Xl IJKT. TIME - 00i57
1003
80.
SO.
40.
20.
A3. 35X5
f\
A1.16X5
A A7.11X4
A A
I \ M AS.83E4
A3. 49X4 i / *\ 1. J L /I A
rJ\ HJ$\Aj^4 J V^/ V *A~sJ\n J\J \A-A -J \~ A_ A
.7.8X4
'.6.2X4
r-4 . 7X4
.3.1X4
.1.6E4
28*, 36 ' '28,48 ' ' 29\00 ' 29*, 13 ' 39*, 24 29\36 ' 29*, 4 8 30>6o' 30tl3 30*, 34 30\36 Tim*
Fil*:S975865 tl-346 Atxjsl3-SXP-1997 00,54,19 XI+ Voltage SIX 70S Hoi** ,5 52
391.8127 F,3 BSOB(356,30,-3.0) PXD(7,5,3,0.05\,2208.0,1.00\,r,T) XxpiEPCDS
TSIAHSLS LABS T*JCt:O-M23-4 TUt4 3057X1 ZWJ. TZNZ - OOs 57
1001
80J
so:
40.
20:
Al .81X5
(\
rt
I A9.16X4
1 1 lil AS. 62X4
A 1
A3.75X47f7x3 A104( 1 I \ A1.SX4 ,a on^^Jy. ,,« f\ A1.59X4
J~J\s*/ WWVAy^A^VA.yVA/ W^W \»XN-M__/L^iAAXNA-~' [ \A^>^Ay \y\^yvAV/>^^AyvA«y
-.5.7X4
.4.5X4
.3.4X4
.2.3X4
'.1.1X4
28\36 28*, 4 8 39*, 00 29,12 29\24 29*, 36 29*48 3o',00 30,12 3o',24 30t36 Tim*
Til*,S975865 tl-346 Aim»,848
401.8558 Fi3 BSO*(256,30,-3.0) PXD(7,5,3,0.05\,3393.0,1.00\,r,T) XxpiXPCUS
TRIANGLE LABS T*xtiO-M23-4 TLH43057X1 UKT. TIMS - 00»57
1001
80.
so:
*°-.
20-
0'
A3. 21X7
A A2.16E7
A A
ft
V
/ f \ 1 \
-9.8X6
.7.8X6
.5.9X6
.3.9X6
.2.0X6
o.oxo
28*: 36 28*, 4 8 29,00 29*, 12 29t24 29,36 29,48 30tOO ' 30*, 13 ' 30\24 ' 30*, 36 ' Tim*
File, 3975865 fl-346 Acq:13-SXP-1997 00, 54, IS EI+ Voltage SIX 70S Xoim*t792
403.8529 T:3 BSOB(256,30,-3.0) PXD(7,5,3,0.05\,3168.0,1.00\,r,T) XrptXfCOS
TXIANGLX LABS T»xtiO-M33-4 TLH43057X1 1X7. TIME - 00:57
1001
80.
SO.
40^
30.
0"
A1.79X7
([ A1.74X7
A l\
ft
V
/ I \ 1 \
-7.8X6
.6.2X6
.4.7X6
.3.1X6
.1 . 6X6
O.OT.O
28*, 36 28\48 29*, 00 29*, 12 29*, 24 39\36 29*: 4 8 ' 30*00 ' 30*, 12 ' 30t24 ' 30*, 36 ' Tim*
Tll»iS975865 tl-346 Aoqtl3-SXP-1997 00 1 54, 19 XI+ Volt*g» SIX 70S -^
392.9760 r,3 XipiXPCUS
TJtlANGLS LABS T»xtiO-M23-4 TLH43057X1 UKT. TOtX - 00t57
1001
80.
SO.
40.
20.
0.
28'37 "A?3 32\? t^ 29,16 39i33 a9'57 30, 0630'13 30t3i 30'31
./A A -r, / \kf\ J \t\. l\ . X. i 29 1 28 rvwV-vA. N\ LST\A/\ » AA^ A«/>A—
/yvw^v v^v w\^/\»*ffiqr*r~>^
\l '
-.4.7X6
.3.8X6
.2.8X6
.1.9X6
.9.4X5
0.0*0
75
-------
r±le>S975e65 #1-390 Aog,13-SEf-1997 OOiS4:19 EI+ Voltage SIS 70S Hoi*o:1555
407.7819 Tt4 BSUB(256,30,-3.0) PXD(7,5,3, 0.05%, 6220. 0,1.00\,e,T) XxptXPCDS
TRIANGLE LASS T*xt,O-M23-4 TLIf43057Sl HIT. TIMX - 00(57
1001 A2.87S5
31:48 32i00 32,12 33,24 32,36 32,48 33tOO 33,22
rll»,S975865 fl-390 Acq,13-SXP-1997 00,54,19 XI+ Voltag» SIS 70S Wbi«ail505
53 F,4 BSUB(256,30,-3.0) PKD(7,5,3,0.05\, 6020.0,1.00\,r,T) ExpiXfCaS
TRIANGLE LABS Ttact,O-M23-4 TLIt43057X1 OCT. TOtf - 00i57
A1.13E5
A2.03E4 .A1.93
31,48 32tOO 32,12 32,24 32,36 32,48 33,00
r±lmiS97S865 fl-390 Aoqtl3-SXf-1997 00,54,19 ZI+ Volt»y» SIX 70S Soi*ut999
409.7789 F,4 BSUB(356,30,-3.0) tXD( 7,5, 3, 0.05%, 3996. 0,1. 00\,T,T) XxptXTCUS
XXIANGZX LABS T»rttO-tt23-4 TLH43057B1 UKT. TOfS - 00,57
33,12
33124
1001
sol
601
401
201
A3.90X5
A9.65E4
AA
A1.36E5
A2.3SX4
A A6.
^^r V\^-v,-^_/
39X4
33,24
1003
80J
40
0:
A9.06E6
AS.86X6
31J48 33,00 33,13 33,34 33,36 33,48 33,00
file,3975865 fl-390 Acq,13-SXP-1997 00,54,19 XI* Valtag* SIS 70S Ifoi*»il083
419.8320 T,4 BSVB(256,30,-3.0) PKD(7,5,3,0.05\,4333.0,1.00\,r,T) XxptXTCOS
TSIA1KLX LABS T»*t,0-M23-4 TLIf430S7Sl XKT. TIME * 00(57
33,12
33124
100]
80:
40:
20:
A2.}5Z7
A1.64X7
31,48 32', 00 32,12 32,24 32,36 32,48 33,00 33,12
,8975865 fl-390 Acqt 13~SSP-1997 00,54,19 EI+ Volttgo SIS 70S
430.9729 T:4 XxpiEPCUS
TRIANGLE LABS Text:0-M23-4 TUt43057Xl INJ. TIME - 00,57
33,24
1003
80J
601
40:
20:
31,50
31,48 33,00 32,12 32,34 33,36 33,48 33,00 33,12
r±lm,S975865 fl-390 Acqil3-SEP-1997 00,54,19 EI+ Volt*gm SIS 70S
479.7165 f,4 SxptEfOJS
TXIAHGLX LABS Tuxt,0-M33-4 TLIf43057Sl HC7. TIME * 00.57
33,24
-1.1X5
-.9.1X4
.6.8X4
.4.5X4
.3.3X4
.0.0X0
-3.6E6
-2.9E6
.1.4X6
-.7.3X5
0.0X0
-8.8X6
.7.1X6
.5.3X6
.3.5X6
'•-1.8X6
0.0X0
3.0X6
.3.4X6
.1.8X6
.1.3X6
.6.0X5
0.0X0
31,48
33,00
32,12
33,34
33,36
33,48
33100
33113
33134
76
-------
•J.1OISS75865 tl-iSO ACqiJ.J-SEf-J.S9/ OOtHlJ.9 SI+ Valtfg* SIX 70S MOi*»:3304
423.7766 T>4 SSOS(256,30,-3.0) PXD(7,5,1,0.05%, 8816.0,1. 00\,r,T) XrptXPCOS
TRIASGLE LASS T*xt:O-M23-4 TLIt43057Xl IXT. TIMS - 00»57
1004 A3.22X5
32:00 32t06 32:12 32tli 32>24 32i30 32:36 32*43 32:48 32:54 33.00
Til»:S975865 tl-390 Acq*13-SXf-1997 00:54:19 EH- Voltag* SIX 70S Hoi»»*1035
425.7737 T:4 SSV3(256,30,-3.0) fXD(7,5,3,0.05\,4140.0,1.00\,r,T) ExptEPCUS
TXIASGLX LASS T&zt:0-M23-4 TLH43057X1 XK7. TIME - 00:57
100A A1.75E5
0.0X0
33:06 33:12 Time
32:00 32*06 32:12 32:18 32:24 33*30 33*36 32*42 32*48 32*54 33*00
ril»iS975865 tl-390 Acq:13-SEf-1997 00*54*19 EI+ Voltag* SIX 70S Hoi***400
435.8169 T*4 SSUS<256t30,-3.0) PB>(7,5,3,0.051,1600.0,1.00\,T,T) XxptXfCOS
TXIAHGLX LASS Tait:O-H23-4 XLIt43057Xl OUT. TIME - 00*57
1001 A1.45E7
so:
SO.
40.
20.
32:00 32:06 32:12 32il8 32*24 32*30 32*36 33*43 33*48 32:54 33*00
rile:S975B65 tl-390 Acqtl3-SEf-1997 00i54:19 EI+ Voltage SIX 70S No±mut353
437.8140 r*4 BSUZ(256,30,-3.0) PKD(7, 5, 3, 0 .05\, 1413.0,1 .00\,r,T) ExpiKPCUS
TRIANGLE LASS Text:O-H23-4 TLH43057X1 INT. TIMS * 00:57
.0.0X0
33:06 33:12 Tim*
-5.8X6
.4.7X6
.3.5X6
.2.3X6
.1.2E6
10 0\
BO:
eo:
40.
20:
o:
A1.J1E7
-5.6X6
.4.5X6
.3.4X6
'.2.2X6
'.1.1X6
32*00 32*06 32*12 32:18 32*24 32:30 32*36 32*42 32:48
ril«*S975865 tl-390 Acq*13-SXP-1997 00:54:19 EI+ Voltagv SIS 70S
430.9739 T*4 ExptEfCUS
TXIAHGLX LASS T*rttO-M23-4 TLII43057X1 IKT. TIME ' 00(57
18
33*54 33*00 33*06 33*13
0.0X0
Tim.
33*08
80.
so:
40.
20:
o:
,3.0X6
'.3.4X6
.1.8X6
.1.2X6
'.6. 0X5
32:00 32*06 33*13 32*18 33*34 33*30 33*36 33:42 32*48 32:54 33:00
. f 0 flrn
33«0tf 33:12 Tlmm
77
-------
.?....?....?....?....?...g 2 !• t
igggggggggg
00
-------
File
457.
TXIA
1003
so:
eo:
40:
20:
rile
459.
TXIA
1001
so:
eo:
40:
20:
rile
469.
TXIA
1003
so:
60.
40.
20.
rile
471.
TXIA
1001
80.
so:
40.
20:
0
File
430.
TXIA
1001
80.
60.
40.
20.
0
IS975865 il-390 Acqtl3-SEP-1997 00>54il9 XI* Voltage SIX 70S BoimetlOl
7377 Fs4 BSOB(256,30,-3.0) PKD(7,5,3,0.05\,404 .0,1.00\,F,T) XiptXPCVS
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35:12 '35il8 35', 24 3s', 30 '35t36
,3975865 il-390 Acqtl3-SXP-1997 00,54:19 XI+ Voltage SIX 70S Hoime:63
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IfSLX LABS TmrttO-M23-4 TLH43057X1 UKT. TIMX -
35:13 35*18 35:34 35\30 35\36
,3975865 il-390 Acqtl3-SXP-1997 00:54:19 XI+ Voltagw SIX 70S Hoimet52
7750 Fi4 BSUB(256,30,-3.0) PXD(7,5,3,0.05\r208.0r1.00\,rtT) XzptXPCUS
NGLS LABS Text.:O-M33-4 TLH43057X1 UKT. TIHX -
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,3975865 il-390 Acqil3-SXP-1997 00:54:19 11+
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,4.1X4
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79
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Channel I 338,9782 Peak top
HelgHt 2,32 volts Span 298 H*
Systet file rate EPOJS2
Data fiUnaie fl:S913971
Resolution 18866
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0 356
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80
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-------
TLI Project: 43057rl
Client Sample: O-M23-4
Method 23 TCDD/TCDF Analysis (DB-225)
Analysis File: P973849
Client Project:
Sample Matrix:
TLI ID:
Sample Size:
Dry Weight:
GC Column:
.teVMcr TLAHT "*"
M23TRAIN
181-27-6A-C
1.000
n/a
DB-225
Date Received: 08/29/97
Date Extracted: 09/06797
Date Analyzed: 09/12/97
Dilution Factor: n/a
Blank File: P973848
Analyst WK
Spike File:
ICal:
ConCal:
% Moisture:
% Lipid:
% Solids:
SPC2NF04
PF22206
P973843
n/a
n/a
n/a
Analytes
\ ;,; ->«&&
««H\ \ t ^ v t "^If^fc y%^'k j ***•"• ** •>3Cfciii3A*w*^ %
Ktl"1 ^ v ' ^ ^ '" %tp-6i?" "'*"* •">\CMw»^%^uv s vj
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2,3,7,8-TCDF
ND
0.01
bttemaf Standarcf
13C,2-2,3,7,8-TCDF
4.1
104
40%-130%
0.76
20:42
Recovery $^o^«j
13C12-1,2,3,4-TCDD
0.81
19:47
Data Reviewer.
Page 1 of 1
09/14/97
C2NF.PSR »iOO. LARS6 IO.M
Triangle Laboratories, Inc.®
801 Capitola Drive • Durham, North Carolina 27713
Phone: (919) 544-5729 • Fax: (919) 544-5491
Printed: 17:55 09/14/9
90
-------
Initial
.Date.,
Data Review By:
\j V Jj/JLll'fj.-^Calculated Noise Area:
The Total Area for each peak with an ion abundance ratio outside
ratio limits has been recalculated according to method requirements.
2.55
Page No.
09/14/9"
Listing of P973849B.dbf
Hatched GC Peaks / Ratio / Ret. Time
Compound/
M_Z.... QC.Iiog Omit '.-toy ..RT. OK Ratio Total .Area... Area.Peak.1. . Area. Peak. 2.. Rel.RT Compound. Name.. ID.. Flags.
TCDF
304-306
D
304-306
13C12-TCDF
316-318
316-318
13C12-TCDD
332-334
0.65-0.89
DC
DC
DC
DC
DC
DC
DC
DC
DC
DC
DC
DC
DC
d
DC
DC
DC
DC
DC
DC
DC
DC
DC
DC
DC
DC
DC
DC
DC
DC
NL
SH
SN
SN
SN
SN
SN
SN
SN
SN
SN
SN
SN
SN
SN
SN
SN
SN
SN
SN
SN
SN
0
NL
WL
WL
SN
SN
SN
WH
2
NL
0:
18:
00
17
18:22
18:
18:
18:
18:
19:
19:
19:
19:
20:
20:
32
38
43
51
27
46
58
59
03
14
20:43
20:48
20:56
20:59
21:
21
21
21
22
:22
:28
:50
:57
:12
RO
RO
RO
RO
RO
RO
RO
RO
RO
RO
RO
RO
RO
RO
RO
RO
RO
RO
RO
RO
0.
2.
1.
2.
0.
2.
0.
1.
0.
0.
0.
0.
0.
0.
1.
0.
1.
0.
0.
3.
4.
0.
75
67
31
68
22
04
13
02
31
29
27
39
24
92
11
61
46
64
85
11
88
28
Peaks
0:00
19
19
20
20
20
21
21
22
:01
:26
:17
:42
-.52
:02
:14
:35
0.
RO
RO
RO
1.
0.
0.
0.
0.
0.
0.
3.
0.
0.
0.
0.
0.
6.
1.
2.
77
85
57
78
44
41
28
10
94
46
60
25
80
94
15
32
0.46
1.86
0.72
0.
0.
.34
.57
0.34
0.
.00
65-0.89
0.
1.
0.
3.
97
.25
,78
.24
0.76 1
RO
RO
RO
0.
0.
1.
0
Peaks
0
18
19
19
:00
:28
:33
:47
0.
RO
.26
.63
.11
.85
1
65-0.89
1
0
0
0
.58
.67
.79 1
.81 1
2,
1
.09
.15
6.21
0
,768
1
0
5
14
.65
.72 763.37
.38
.90
.45 3.43
.24
0.786-1.096
0.
0.
0.
0.
0.
0.
0.
000
883
887
895
900
904
911
0.940
0.
0.
0.
0.
0.
1.
1.
1.
1.
1.
1.
955
965
965
969
977
001 2378-TCDP AN
005
Oil
014
032
.037
1.055
1.
.060
1.072
0.952-1.048
0,
0,
0
0
1,005.35 1
1
1
3.08 1
1
.000
.919
.939
.980
.000 13C12-2378-TCDP ISO
.008
.016
.026
.091
,774.17
1
5
,310
,229
.50
.39 2.16
.93 576.92
.21 550.46
0.897-1.103
0
3.23 0
734.01 1
678.75 1
.000
.945
.000 13C12-2378-TCDD IS1
.012 13C12-1234-TCDD RSI
Triangle Laboratories, Inc.® Analytical Services Division
501 Caprtola Drive • Durham, North Carolina 27713
'hone: (919) 544-5729 • Fax: (919) 544-5491
Printed: 17:55 09/14/97
91
-------
rage No. 2 Listing of P973849B.dbf
39 U-97 Matched GC Peaks -' Ratio / Ret. Time
Compound/
M_Z.... QC.Log Omit Why ..RT. OK Racio Total.Area... Area.Peak.1.. Area.Peak. 2.. Rel.RT Compound.Name.. 1C.. Flags.
DC SN 19:55 RO 1.02 1.65 1.019
DC SN 20:01 RO 0.34 0.53 1.024
20:25 RO 0.93 16.78 8.78 9.48 1.044
DC SK 20:57 RO 0.36 1.72 1.072
DC SN 21:08 RO 0.62 0.78 1.081
DC SN 21:13 0.73 1.75 1.085
DC SN 21:17 RO 1.37 0.81 1.089
DC WH 21:42 RO 3.11 0.48 1.110
DC WH 21:57 0.68 9.31 1.123
332-334 4 Peaks 2,562.31
Column Description 'Why Code Description QC Log Oesc.
H_Z -Nominal Ion Hass(es) WL-Below Retention Time Window A-Peak Added
. .RT. -Retention Time (mm:ss) WH-Above Retention Time Window K-Peak Kept
Rat.l -Ratio of H/M+2 Ions SN-Below Signal to Noise Level D-Peak Deleted
OK -RO*Ratio Outside Limits
-------
File:P973B49 tl-755 Acq:12-SEP-1997 15l53s55 BI+ Voltage SIM 7Of Hoifas37B
303.9016 BSUB(256,30,-3.0) PKD(5,3,1,0.101,1512.0,0.00\,F,r) XxptDB225
TRIANGLE LABS rext:0-M2J-4 TLH43057R1
1001 A3.61X4
17': 00 18'tOO 19:00 20tOO 21*00
ril»,P973849 tl-755 Aoqtl2-8XP-1997 15:53:55 EI+ Voltaga SIX 70P Bo±**i506
305.8987 BSOS(256,30,-3.0) PKD(S,3,1,0.10\,2024.0,0.00\,T,T) XxptDB22S
TRIANGLE LABS TmxttO-M23-4 TLIt43057Sl
1004
32 tOO
17': 00 IStOO 19100 20iOO 21iOO
r±l»0-M23-4 XLII43057X1
100% A7.f3X6
so:
so:
40:
22100
01
17,00 18,00 19,00 20,00 21,00
ril»tP973849 tl-755 Aoqil2-SXP-1997 15,53,55 XI+ Volt*g» SIX 70P BoifmtSBB
317.9389 BSOB(256,30,-3.0) PXD(5,3,1, 0.10\,2352.0,0.00\,T,T) XxptDB225
TXIAWSLX LABS Ttxtl0-H23-1 XLI143057X1
100\ A1.01E7
801
60'.
40:
201
01
22,00
17,00 18,00 19,00 20,00 21,00
ril»,P973849 tl-755 Acq, 12-SEP-1997 15,53,55 EI+ Volt*g» SIX 70P
375.8364 Exp,DB225
TSIANGLS LABS TfXttO-M23-4 TLIt43057Xl
10 0\ 16129
22,00
17100
18,00
19100
20100
21>00
-2.0X6
.1.6X6
.1.2*6
.8.2X5
.4.1X5
0.0X0
££••
-2.7X6
.2.1X6
.1. 6X6
.1.1X6
.5.3X5
0.0X0
T±m»
22,00
93
-------
'H»iPS73a49 tl-755 AcxjllJ-SEF-1397 15i53i55 Sl-r- VolCMfff SIX 70P Hoif»tjBB
319.8965 BSUB(356,30,-3.0) PJO>(5, 3,1, 0.10\,1552. 0, 0.00\,T,T) EiptDB225
TRIANGLE LABS TfXttO-H23-4 TLIt430S7Xl
1001 A1.2BE4
80.
18100 19,00 20tOO
r±l*iP973849 tl-755 Aoqil3-SEP-1997 IStSStSS EH- Voltag» SIX 7OP Soit»,499
321.8936 BSUB(256,30,-3.0) PKD(5,3,1, 0.10\, 1996.0, 0.00\,T,T) EiptDB225
TRIANGLE LABS Text:0-H23-4 XLIt43057Kl
100% A4.38E3
18'tOO IS'iOO 20iOO 21100
r±lutP973849 tl-755 Aoytl3-SXP-1997 15>53t55 XI+ Volttgm SIS 7OP Hoi»mt366
327.8847 BSUB(256,30,-3.0) PKD(S,3,1,0.10\,1464 .0,0.00\,T,T) ElpiDB225
XRIASGLX LABS T*xt,0-K23-4 TLH430S7X1
1004 A1.10C7
so:
40.
20:
18:00 19,00 20(00 21iOO
Til9iP973849 tl-755 Ac?tl3-SXP-1997 15t53tS5 XI+ VoltMgm SIX 70P Solf»t€69
331.9368 BSOB(256,30,-3.0) PKD(5,3,1,0.101,2676.0,0.00\,r,r) ExpsDB225
TRIANGLE LABS TaxttO-M23-4 TZ.H43057S1
1004 A5.50E6
22,00
80.
60.
40.
20.
0.
AS.77X6
16i00 19,00 20,00 31tOO
ril»tP973849 tl-755 Aoqtl3-SSP-1997 15,53,55 EI+ Voltagre 3IS 70P Koim»t427
333.9338 BSUB(256,30,-3.0) PKD(5,3,1,0.10\,17QS.0, 0. 00\,T,T) Ezp,DB225
TRIANGLE LABS TmxtiO-H23-4 TLH43057X1
1001 A6.79X6
22 i 00
80.
60.
40.
20.
A7.34X6\
.1.7X6
.1.2X6
.8.3X5
'.4.1X5
.0.0X0
Tin*
_1.5r6
'.1.2E6
.9.1X5
.6.0X5
.3.0X5
0. 0X0
Tim,
.1.8X6
.1.4X6
.1,1X6
.7.2X5
.3. 6X5
18,00
19,00
20100
21:00
22100
0.0X0
TlM
94
-------
rilesP973849 tl-755 Acqtl2-SEP-1997 15(53(55 EH- Voltmgm SIX 70P
303.9016 EipiDB335
TRIANGLE LABS T»xt:0-M23-4 XLIt43057Xl
1004 20f43
17\00
18'tOO 19iOO 20:00 ' ' 21 i 00
r±laiP973849 tl-755 Aoqil3-SXP-1997 15t53»5S XI+ Volt»gm SIM 70P
315.9419 ExptDB335
TRIANGLE LABS T*XttO-M23-4 TLIt43057Xl
1001
sol
sol
40l
aol
i7:ob18106 19:00 aotoo ait oo
FilatP973849 fl-755 Acqtl3-SXP-1997 15i53i55 XI* Voltage SIX 70P
319.8965 KipiDBaaS
TXIANGLX LABS Tflt:0-M23-4 TLIt43057Xl
aaioo
22100
17100 18'tOO 19'tOO 20>00 21100
TileiP973849 #1-755 Acq:12-SKP-1997 15i53s55 EI+ Voltaya SIX 70P
331.9368 Zrp,DB225
XSIANGLX LABS TexttO-H23-4 TLH43057S1
1001
aol
sol
4ol
aol
17:00 18:00 19(00 20(00 21:00
Fll«iP973849 tl-755 Acq:12-SEP-1997 15(53:55 XI* Vbltaga SIX 70P
293.9835 XxptDB335
TBXANGLX LABS Taxt,0-M23-4 TLIt43057Xl
i7t43 1B*26 19,21 19,51 30,22 21(08
80J
sol
401
aol
33100
17,00 18,00 19,00 20(00 21(00
Til»tP973849 tl-755 Aoq,13-SXP-1997 15(53(55 XI+ Voltmg* SIX 70P
330.9793 Xxp,DB225
TXIAXGLX LABS T»xtiO-M23-4 TLIt43057Xl
100* .... 19,23 30*24 21i
, ^ 16,44 17,22 17(50 1Bt35
80:
so.
401
aol
ol
22(00
.1.6X6
.1.2X6
.8.2X5
.4.1X5
0.0X0
,.1.5X6
.1.3X6
.9.1X5
.6.1X5
.3.0X5
0.0X0
lima
-7.2X6
.5.7X6
.4.3X6
.2.9X6
.1.4X6
,0.0X0
TiM
,.7.4X6
.5.9X6
.4.5X6
.3.0X6
.1.5X6
17100
18(00
19,00
20100
21100
22(00
0.0X0
TlM
95
-------
fl:P973849
Ref, lass 292,9925 Peak top
Heloht 1,14 volts Span 296 ppi
Systa file nae
Data fiLenaae
Resolution
Group nuiber
loniiatlon wde
Switching
Ref, lasses 292,9825,
fl 292.9625
B 383.9816
D 315,3419
E 317,9389
F 319.3965
G 321,8936
H 327,8847
I 338,9792
J
K
L
H
1
El*
VOLTAGE
388,3761
338,9792
331,9368
£5,8364
Channel I 338,9792 Peak top
Helpjt 1.12 volts Span 208 ppi
96
-------
I-
O5
File:P973B49 #1-755" Acq; 12-5EP-1997 15:53:55 EI+ Volhage SIR TOP
303.9016 Exp:DB225
Sample Text:0-M23-4 TLI#43057Rl File Text:0-M23-4 TLI#43057R1
100% 20:43
19:00 20:00 21:00 22iOO
File:P973849 #1-755 Acq:12-SEP-1997 15:53:55 EI+ Voltage SIR 70P
305.8987 Exp:DB225 \fC
Sample Text:0-M23-4 TLI#43057Rl File Text:0-M23-4 TLI#43057R1
100%
80j
23:00
.O.OEO
Time
19:00 20:00 21iOO 22iOO
File:P973849 #1-755 Acq:12-SEP-1997 15:53:55 EI+ Voltage SIR 70P
315.9419 Exp:DB225
Sample Text:0-M23-4 TLI#43057Rl File Text:0-M23-4 TLI#43057R1
100% 20;42
80.:
60J
40J
20-
OJ
2300
'igloo'
20:00
1 1 '
21:00
22:00
23:00
JiO.OEO
Time
2.1E6
L1.6E6
L1.2E6
L8.2E5
_4.1E5
O.OEO
Time
-------
CALIBRATION
DATA
Triangle Laboratories, Inc.
801 Capitols Drive P.O. Box 13485
Durham, NC 27713-4411 Research Triangle Park, NC 27709-3435
919-544-5729 Fax # 919-544-5491
98
-------
Continuing calibration tor P973843
Analysis Date : 09/12/97
Operator : WK
Init Calibration.: PF22206
ICal Date : 02/20/96
Analysis Time....: 11:04
Analyte Sumnary
Name
2378-TCDF
TOTAL TCDF
2378-TCDD
TOTAL TCDD
RF Ratio
RT
Method : C2NF
Instrument..: P
Std.Conc : 5.00
GC Column...: DB-225
ICal Delta
RT Rel. RT RF RF %D
1&2 Lo/High
0.964 0.76 16:14 20:40 1.0008 1.040 -0.076 -7.3%
22:38
0.964 0.76 1.040 -0.076 -7.3%
1.001 0.75 17:03 19:28 1.0009 0.992 0.009 0.9%
22:00
1.001 0.75 0.992 0.009 0.9%
Other Standard Sunmary
Name RF Ratio
1&2
37C1-TCDD 0.937
ICal Delta
RT RT Rel. RT RF RF %D
Lo/High
17:27 19:28 1.0009 1.014 -0.077 -7.6%
21:27
Internal Standard Sunmary
Name RF Ratio
162
13C12-2378-TCDF 1.201 0.77
13C12-2378-TCDD 1.006 0.79
ICal Delta
RT RT Rel. RT RF RF %D
Lo/High
19:39 20:39 1.0000 1.388 -0.187 -13.5%
21:39
17:27 19:27 1.0000 1.067 -0.061 -5.7%
21:27
Recovery Standard Sunmary
Name RF Ratio
142
13C12-1234-TCDD 1.000 0.82
ICal Delta
RT RT Rel. RT RF RF %D
Lo/High
19:41 1.0120 1.000 0.000 0.0%
Page
'riangle Laboratories, Inc.® Analytical Services Division
01 Caprtola Drive • Durham, North Carolina 27713
'hone: (919) 544-5729 • Fax: (919) 544-5491
Printed: 11-.4609/12/97
-------
Date: 09/12/97
TRIANGLE LABORATORIES, INC.
Continuing Calibration for S975861
Operator
• ML
/ •* '
Init Calibration.: SF56117
ICai Date
Analyte Summary
Name
Total MCDF
Total MCDD
Total DCDF
Total DCDD
Total TriCDF
Total TriCDD
2378-TCDF
TOTAL TCDF
2378 -TCDD
TOTAL TCDD
12378-PeCDF
23478- PeCDF
TOTAL PeCDF
12378-PeCDD
TOTAL PeCDD
123478-HxCDF
123678-HxCDF
234678-HxCDF
123789-HxCDF
TOTAL HxCDF
123478 -HxCDD
123678-HxCDD
• 06/10/97
RF Ratio
0.000
0.000
0.000
0.000
0.000
0.000
1.182
1.182
1.078
1.078
1.051
1.100
1.075
1.210
1.210
1.070
1.354
1.059
0.981
1.116
0.908
1.059
1&2
0.81
0.81
0.79
0.79
1.53
1.52
1.52
1.59
1.59
1.33
1.31
1.32
1.34
1.33
1.25
1.25
r««^h>«AWU . . .
Instrumer
Std.Conc
RT RT Rel. RT
Lo/High
1:34
15:34
2:19
16:19
8:34
16:34
9:19
17:19
12:34
19:34
14:19
20:19
18:05 21:35 1.0008
23:33
19:31 22:20 1.0007
23:32
23:27 25:38 1.0007
27:30
26:22 1.0293
24:45 26:43 1.0000
27:22
28:02 29:09 0.9971
30:42
29:15 1.0006
29:45 1.0177
30:27 1.0416
28:32 29:52 0.9972
30:23
29:57 1.0000
Page 1
.... .1* .j i
it . . : S
...• 50 00
ICai Delta
RF RF %D
2.087 -2.087 100.0%
1.625 -1.625 100.0%
0.687 -0.687 100.0%
1.326 -1.326 100.0%
1.082 -1.082 100.0%
0.933 -0.933 100.0%
1.251 -0.069 -5.5%
1.251 -0.069 -5.5%
1.191 -0.113 -9.5%
1.191 -0.113 -9.5%
1.111 -0.060 -5.4%
1.115 -0.015 -1.4%
1.113 -0.038 -3.4%
1.256 -0.046 -3.7%
1.256 -0.046 -3.7%
1.215 -0.145 -11.9%
1.574 -0.220 -14.0%
1.247 -0.188 -15.1%
1.105 -0.124 -11.2%
1.285 -0.169 -13.1%
0.953 -0.045 -4.7%
1.133 ^0.074 -6.6%
Triangle Laboratories, Inc.® Analytical Services Division
801 Capitota Drive • Durham, North Carolina 27713
Phone: (919) 544-5729 • Fax: (919) 544-5491
Printed: 22:27 09/12/97
100
-------
ate: 09/12/97
TRIANGLE LABORATORIES. INC.
Continuing Calibration
23789-HxCDD
OTAL HxCDD
234678-HpCDF
234789-HpCDF
OTAL HpCDF
234678-HpCDD
OTAL HpCDD
CDF
CDD
1
1
1
1
1
0
0
1
1
.090
.019
.503
.267
.385
.934
.934
.597
.040
1.25
1.25
1.03
1.03
1.03
1.00
1.00
0.86
0.85
31:44
33:15
31:59
32:54
31:16
39:16
31:16
39:16
30:14
31:54
33:05
32:44
35:25
35:17
for S975861
1 . 0095
1.0000
1.0371
1.0000
1.0043
1.0005
ther Standard Summary
ante
7C1-TCDD
3C12-PeCDF 234
3C12-HXCDF 478
3C12-HXCDF 234
3C12-HXCDF 789
3C12- HxCDD 478
3C12-HpCDF 789
nternal Standard
ame
3C12-2378-TCDF
3C12-2378-TCDD
3C12-PeCDF 123
3G12-PeCDD 123
3C12-HXCDF 678
JC12- HxCDD 678
0
0
0
0
0
0
0
RF
.842
.975
.934
.903
.789
.950
.830
Ratio
162
1.54
0.50
0.49
0.49
1.21
0.42
RT
Lo/High
20:19
24:19
21:37
29:37
29:54
35:54
RT
22:20
26:21
29:09
29:44
30:27
29:52
33:04
Rel. RT
1.0007
1.0286
0.9971
1.0171
1.0416
0.9972
1.0366
Summary
1
1
1
0
1
0
RF
.488
.131
.302
.780
.171
.934
Ratio
162
0.76
0.80
1.53
1.52
0.50
1.21
RT
Lo/High
20:34
22:34
20:19
24:19
21:37
29:37
22:43
30:43
25:14
33:14
28:57
30:57
Page
RT
21:34
22:19
25:37
26:43
29:14
29:57
2
Rel. RT
1.0000
1.0000
1.0000
1 . 0000
1.0000
1.0000
1.091
1.059
1.543
1.184
1.363
1.068
1.068
1.493
1.105
ICal
RF
0.843
0.970
0.959
0.926
0.805
0.973
0.771
ICal
RF
1.318
1.066
1.133
0.635
1.204
0.995
-0
-0
-0
0
0
-0
-0
0
-0
.001
.040
.040
.083
.022
.134
.134
.104
.065
-0.
-3.
-2.
7.
1.
-12.
-12.
7.
-5.
1%
8%
6%
0%
6ft
6%
6%
0%
9%
Delta
-0
0
-0
-0
-0
-0
0
RF
.001
.005
.025
.023
.016
.023
.059
%D
-0.
0.
-2.
-2.
-2.
-2.
7.
1%
5%
6%
5%
0%
4%
6%
Delta
0
0
0
0
-0
-0
RF
.170
.065
.169
.145
.033
.061
%D
12.
6.
14.
22.
-2.
-6.
9%
1%
9%
9%
7%
1%
angle Laboratories, Inc.® Analytical Services Division
\ Capitola Drive • Durham, North Carolina 27713
one: (919) 544-5729 • Fax: (919) 544-5491
Printed: 22:27 09/12/97
101
-------
Date: 09/12/97 TRIANGLE LABORATORIES, INC.
Continuing Calibration for S975861
13C12-HpCDF 678 0.831 0.42 29:54 31:54 1.0000 0.887 -0.056 -5.3%
35:54
31:44 32:44 1.0000 0.815 -0.029 -3.5%
33:44
35:07 35:16 1.0000 0.519 -0.066 -12.6%
35:27
13C12-HpCDD 678 0.786 1.10
13C12-OCDD 0.453 0.94
Recovery Standard Summary
Name RF Ratio
RT
ICal Delta
RT Rel. RT RF RF
%0
1S2 Lo/High
13C12-1234-TCDD 1.000 0.81
13C12-HXCDD 789 1.000 1.21
22:08 0.9918 1.000 0.000 0.0%
30:14 1.0095 1.000 0.000 0.0%
QC Front End Check:
1.4500
Page
Triangle Laboratories, Inc.® Analytical Services Division
801 Capitals Drive • Durham, North Carolina 27713
Phone: (919) 544-5729 • Fax: (919) 544-5491
Printed: 2227 09/12/97
102
-------
TRIANGLE LASORAICaiES, INC.
Initial Calibration SLL-amarv for S~rill7
Date: 06/10/97
nalysis Date. . . . :
nstrument ...
nalytes
otal MCDF
otal MCDD
otal DCDF
otal DCDD
otal TriCDF
stal TriCDD
378 -TCDF
DTAL TCDF
378-TCDD
3TAL TCDD
2378-PeCDF
3478- PeCDF
DTAL PeCDF
Z378-PeCDD
3TAL PeCDD
Z3478-HXCDF
23 6 78 -HxCDF
!4678-HxCDF
23789-HxCDF
)TAL HxCDF
23478-HxCDD
!3 6 78 -HxCDD
137 89 -HxCDD
HAL HxCDD
134678-HpCDF
134789-HpCDF
)TAL HpCDF
134678-HpCDD
HAL HpCDD
DF
CD
her Standards
Cl-TCDD
C12- PeCDF 234
C12- HxCDF 478
C12- HxCDF 234
C12- HxCDF 789
C12-HXCDD 478
C12-HpCDF 789
ternal Standards
C12-2378-TCDF
C12-2378-TCDD
C12- PeCDF 123
06/10/97
s
2
1
0
1
1
0
1
1
1
1
1
1
1
1
1
1
1
1
1
1
0
1
1
1
1
1
1
1
1
1
1
RF
.087
.625
.687
.326
.082
.933
.251
.251
.191
.191
.111
.115
.113
.256
.256
.215
.574
.247
.105
.285
.953
.133
.091
.059
.543
.184
.363
.068
.068
.493
.105
SD
0.000
0,
.000
0.000
0.
.000
0.000
0.000
0.116
0.116
0.
,231
0.231
0.082
0.061
0.069
0.
0.
0.
0.
0.
0.
0.
0.
0.
0.
0.
0.
0.
0.
0.
0.
0.
0.
RF
0.343
0.970
0.959
0.926
0.805
0.973
0.771
0.
0.
0.
0.
0.
0.
0.
RF
1.318
1.066
1.133
0.
0.
0.
113
113
064
099
069
060
062
067
070
067
067
103
100
095
089
089
131
066
SD
038
030
042
021
044
027
049
SD
065
020
051
%RSO
0%
0%
0%
0%
0%
0%
9%
9%
19%
19%
7%
5%
6%
9%
9%
5%
6%
6%
5%
5%
7%
6%
6%
6%
7%
8%
7%
8%
8%
9%
6%
%RSD
5%
3%
4%
2%
5%
3%
6%
%RSD
5%
2%
5%
Page
Method • vm7
ST
8:15
3:42
10:
11;
13:
:38
:09
:59
14:03
19:43
20:36
24:12
24:
25:
27:
28:
28:
29:
28:
28:
29:
30:
31:
31:
34:
34:
59
22
55
01
32
15
41
46
03
45
57
37
09
03
RT
20:
24:
27:
28:
29:
28:
31:
36
58
55
32
15
40
57
RT
19:
20:
24:
1
43
34
11
RT/LO
0:01
0:34
6:43
7:34
10:43
12:34
15:43
16:34
20:11
21:21
24:01
24:45
26:45
27:36
30:02
30:02
RT/LO
18:34
22:11
28:45
RT/LO
18:43
18:34
20:11
5T/HI
13:43
14:34
14 : 43
15:34
17:43
13:34
23:43
24:34
28:11
29:21
32:01
32:45
34:45
35:36
38:02
38:02
RT/HI
22:34
26:11
34:45
RT/HI
20:43
22:34
28:11
Ratiol Ratio2
2.931
2.827
5.965
1.609
1.025
1.064
0.799
0.799
0.772
0.772
1.552
1.470
1.509
1.526
1.526
1.247
1.260
1.243
1.246
1.249
1.265
1.251
1.233
1.249
1.034
1.080
1.053
0.993
0.993
0.876
0.902
Ratiol Ratio2
1.470
0.518
0.517
0.519
1.241
0.424
Ratiol Ratio2
0.734
0.802
1.447
N
1
1
1
1
1
1
5
5
5
5
5
5
5
5
5
5
5
5
5
5
5
5
5
5
5
5
5
5
5
5
5
H
5
5
5
5
5
5
5
N
5
5
5
igle Laboratories, Inc.® Analytical Services Division
Sapitola Drive • Durham, North Carolina 27713
e: (919) 544-5729 • fax: (919) 544-5491
Printed: 09:49 06/10/97
103
-------
TRIANGLE LABORATORIES INC. Date: 06/10/97
Initial Calibration Summary for SF56117
13C12-PeCDD 123 0.535 0.082 13% 25:21 11:21 29:21 1.461 5
13C12-HXCDF 678 1.204 0.073 6% 28:01 I-^Ol 32:01 0.522 5
13C12-HXCDD 678 0.995 0.017 2% 28:45 '.7-.45 29:45 1.240 5
13C12-HpCDF 678 0.887 0.046 5% 30:45 13:45 34:45 0.429 5
13C12-HpCDD 678 0.815 0.077 9% 31:36 20:36 32:36 1.019 5
13C12-OCDD 0.519 0.080 15% 34:02 32:02 36:02 0.866 5
Recovery Standards RF SD %RSD RT RT/LO RT/HI Ratiol Ratio2 N
13C12-1234-TCDD 1.000 0.000 0% 20:21 0.811 5
13C12-HXCDD 789 1.000 0.000 0% 29:02 1.231 5
•»• End of Report **•
Page
Triangle Laboratories, Inc.® Analytical Services Division
801 Capitola Drive • Durham, North Carofina 27713 Printed: 09:49 teri OT97
Phone: (919) 544-5729 • Fax: (919) 5445491 A J ^
-------
7?.:ANGLS lASCSATORIiS OF RTF. INC.
Imzial Calibration Suamary for ??22206
Dace: ::.20/96
Anaiysis Dace. .. .: 02.1:.' 9 6
: P
Mechod : C2NF
GC Colunr....: DB-225
Analyses
2373-TCDF
TOTAL TCDF
2378-TCDD
TOTAL TCDD
RF 3D %RSB
1.04C 0.109 10*
1.040 0.109 10%
0.992 0.101 10%
0.992 0.101 10%
3T RT/LO RT/HI Raciol
21:32 14:31 25:31 0.767
0.767
20:12 16:11 24:11 0.782
0.782
N
10
10
10
10
Other Standards
37C1-TCDD
RF SD %RSD RT RT/LO RT/HI Ratio! Racio2 N
1.014 0.048 5% 20:12 18:11 22:11 10
Internal standards RF SD %RSO
13C12-2378-TCDF 1.388 0.062 4%
13C12-2378-TCDD 1.067 0.036 3%
Recovery Standards RF SD %RSO
13C12-1234-TCDD 1.000 0.000 0%
*«» End of Report ***
RT RT/LO RT/HI Ratiol Racio2 N
21:31 20:31 22:31 0.753 10
20:11 18:11 22:11 0.786 10
RT RT/LO RT/HI Ratiol Ratio2 N
20:27 0.794 10
Pag,
riangla Laboratories, Inc.® Analytical Services Division
01 Capitofa Drive • Ourham, North Carolina 27713
hone: (919) 544-5729 * Fax: (919) 544-5491
Printed: 23:10
-------
-------
Appendix C.3
Analytical Data
Method 29 Multiple Metals
-------
-------
CASE NARRATIVE
Analysis of Samples for the Presence of Trace Metals
Method 29 April 1996 Rev.
Client:
Pacific Environmental Services
TLI Project Number: 43377
Date: November 3,1997
This report should only be reproduced in full.
Any partial reproduction of this report requires permission from
Triangle Laboratories. Inc.
Rev. 07-May-97
Triangle Laboratories, Inc.
801 Capitals Drive P.O. Box 13485
Durham, NC 27713-4411 Research Triangle Park, NC 27709-3485
919-544-5729 Fax # 919-544-5491 *
-------
Triangle Laboratories, Inc. November 3,1997
Case Narrative TLI Project*: 43377
Overview
Six train samples and a blank train sample were analyzed for silver (Ag), arsenic (As),
barium (Ba), beryllium (Be), cadmium (Cd), cobalt (Co), chromium (Cr), copper (Cu),
manganese (Mn), nickel (Ni), phosphorus (P), lead (Pb), antimony (Sb), selenium (Se),
thallium (Tl), zinc (Zn), and mercury (Hg). For all analyses, the samples and associated
QC samples were prepared and analyzed following the guidelines of Method 29 April
1996 Rev. Results reported relate only to the items tested.
PC Remarks
The release of this set of data by Triangle Laboratories, Inc. was authorized by the Quality
Control Chemist who has reviewed each sample data package individually following a
series of inspections/reviews. When applicable, general deviations from acceptable QC
requirements are identified below and comments are made on the effects of these
deviations upon the validity and reliability of the results. Specific QC issues associated
with this particular project are:
Sample Receipt:
Seven train samples were received at 22°C on September 24,1997 in good condition. The
samples arrived without coolant, which resulted in the high temperature. Sample O-M29-FB-
HC1 was listed on the client's chain-of-custody, but was not received. The project was
processed without this sample.
Sample Preparation:
Laboratory documentation of the sample preparation is included in the data package.
Instrumentation:
Silver (Ag), arsenic (As), barium (Ba), beryllium (Be), cadmium (Cd), cobalt (Co),
chromium (Cr), copper (Cu), manganese (Mn), nickel (Ni), phosphorus (P), lead (Pb),
antimony (Sb), selenium (Se), and zinc (Zn) concentrations were determined by
Inductively Coupled Plasma Emission Spectroscopy (ICP).
Thallium (Tl) concentrations were analyzed by Graphite Furnace Atomic Absorption
(GFAA).
Mercury (Hg) concentrations were determined by Cold Vapor Atomic Absorption
(CVAA).
2
-------
Triangle Laboratories, Inc. November 3,1997
Case Narrative TLI Project*: 43377
The linear range for the instrument TJA 6 IE Trace Analyzer was based on four standards
and a blank, which established a correlation coefficient value greater than or equal to
0.995. A calibration curve, based on a blank and one standard, is established for each
analytical run, followed by a check high standard and an initial calibration verification
(ICV). The check high standard does not deviate from the calibration curve by more than
5%. In addition, continuing calibration verifications (CCVs) are performed throughout
the analytical run.
A Reporting Detection Limit (RDL) is used instead of an Instrument Detection Limit
(IDL). The spectrometer and atomic absorption instruments can achieve low detection
limits between 0.2-8 ppb levels for many analytes. Triangle Labs is using RDL values of
1-10 times the IDL as detection limits for reporting purposes.
Data Review:
All analytes found in the method blank (MB) are detected at a level equal to or less than
the respective Reporting Detection Limits (RDLs) except for Pb. The following guidelines
may be used to assess analyte concentrations relative to the method blank: 1. Analyte
quantitations should be considered valid if die level of blank contamination is less than five
percent of the level detected in the field sample, 2. Analyte quantitations should be
considered estimated if the analyte level in die sample is five to twenty times the level of
the analyte in the blank, or 3. Analytes whose level in a sample is the same as or less than
five times the level detected in the associated blank should be considered present likely
due to laboratory contamination and not native to the sample. Please note that the Pb
results that are near the RDL should be considered biased low.
All samples were received outside of the 28 day sampling to analysis holding time for Hg,
therefore the holding time for Hg could not be met. All samples were analyzed within the
six month sampling to analysis holding time for all other requested analytes.
The sample IDs on the client chain-of-custody did not match with the IDs on the sample
containers. The sample IDs on TLTs chain-of-custody matches the IDs on the sample
containers. The sample IDs on the Hg spreadsheets for the KMnO4 and HQ containers do
not have the addition description added in order to alleviate redundancy.
The concentrations for Tl demonstrated high negative numbers for the samples analyzed
by ICP, therefore the samples were analyzed by GFAA in order to obtain better results. A
duplicate analysis is not reported for elements analyzed by GFAA. The GFAA instrument
analyzes two separate aliquots of the sample and averages the values for a final result.
These two analyses agree within a RPD of 20% or a second run is done for that sample.
The ICP instrument analyses one continuous aliquot three times and averages the values
for a final result. The ICP does not take two separate aliquots, therefore a DA is
performed.
-------
Triangle Laboratories, Inc. November 3,1997
Case Narrative TLI Project*: 43377
The post-digestion spike (PDS) for Tl for the sample 0-M29-1-FHACEJ;HAIU;ILTER
FH demonstrated a percent recovery outside the QC criteria of 75-125 percent. This result
for the front half post-digestion spike (PDS) indicates significant matrix effects specific to
this analyte in the native sample matrix. The interference QC analysis is not reported (i.e.
MS, MSD, PDS, and serial dilution) for this analyte for the front half samples since the
Method of Standard Additions (MSA) was performed. The MSA results are reported if
the correlation coefficient value is at least 0.995. The MSA results were reported for all
of the front half samples except sample I-M29-1-FHACTJ:HARJFILTER FH. This
sample was analyzed two times and the correlation coefficients for both runs were less
than 0.995, therefore the results for this sample were taken from ICP.
The serial dilution fesults for Cr for the sample O-M29-1-FHACE,FHARJTLTER FH
demonstrated a RPD outside the QC control criteria of 10.0 percent, which indicates the
presence of an amount of interferents specific to this analyte in the native sample matrix.
Please note that the post-digestion spike (PDS) for Cr demonstrated a percent recovery
within QC criteria, which indicates no significant amount of interfences specific to this
analyte in the native sample matrix. Also note that this sample should be considered
biased low for Cr due to matrix interferences.
The serial dilution results for MnJP, Pb, and Zn for the sample O-M29-1-
FHACE,FHAR,FILTER FH demonstrated RPDs slightly outside the QC control criteria
of 10.0 percent, which does not indicate the presence of a significant amount of
interferents specific to these analytes in the native sample matrix. Please note that the
post-digestion spike (PDS) for Pb and P demonstrated percent recoveries within QC
criteria, which indicates no significant amount of interfences specific to these analytes in
the native sample matrix.
The post-digestion spike (PDS) for Be and Pb for the sample O-M29-1-
FHACE,FHAR,FILTER FH and for Mn for sample 0-M29-1-HNO3 BH demonstrated
percent recoveries outside the QC criteria. These results may indicate significant matrix
effects specific to these analytes in the native sample matrix. Please note that sample O-
M29-1-FHACE,FHARJ7ILTER FH should be considered biased low for Be and Pb due to
matrix interferences. Also note that sample O-M29-1-HNO3 BH should be considered
biased low for Mn due to matrix interferences.
The post-digestion spike (PDS) for Ag, P, and Se for the sample O-M29-1-
FHACE,FHAR,FILTER FH and As for sample O-M29-1-HNO3 BH demonstrated
percent recoveries slightly outside the QC criteria, but does not indicate any significant
matrix effects specific to these analytes in the native sample matrix.
The recoveries for the post-digestion spike (PDS) are not reported for Ba, Mn and Zn for
sample O-M29-1-FHACE',FHAR,FILTER FH. The spike concentrations added were
insignificant in comparison to the levels of these analytes present in the native sample.
-------
Triangle Laboratories, Inc. November 3,1997
Case Narrative TLI Project*: 43377
The pre-digestion'spike (MS) and the pre-digestion spike duplicate (MSD) for Hg for the
samples O-M29-1-HNO3 BH, 0-M29-3-HNO3 BH, and O-M29-4-HNO3 BH
demonstrated percent recoveries outside the QC criteria, which may indicate significant
matrix effects specific to this analyte hi the native sample matrix. Please note that these
samples should be considered biased low for Hg due to matrix interferences.
QC requirements:
The duplicate analyses for analytes analyzed by ICP cannot be considered valid qualifiers if
the concentrations of the analytes in the original and/or duplicate sample are not at least
ten times the respective RDLs. The RPDs for these analyses are indicated by or "
-------
Triangle Laboratories, Inc. November 3, 1997
Case Narrative TLI Project*: 43377
By our interpretation, the analytical data in this project are valid based on the guidelines of
Method 29 April 1996 Rev. Any specific QC concerns or problems have been discussed in
the QC REMARKS section with emphasis on their effect on the data. Should Pacific
Environmental Services have any questions or comments regarding this data package,
please feel free to contact Project Scientist, Rose West, at (919) 544-5729 ext.270.
For Triangle Laboratories, Inc.,
Report Preparation Quality Control
Linda F.Jones S?ffy ?
Report Preparation Chemist Report Preparation Chemist
The total number of pages in this data package is:
fllk
/Tr
-------
TRIANGLE LABORATORIES, INC.
LIST OF CERTIFICATIONS AND ACCREDITATIONS
ENVIRONMENTAL
American Association for Laboratory Accreditation. Accredidation pending. Certificate
Number 0226-01. Accreditation for technical competence in Environmental Testing.(lnduding
Waste Water, Sol/Haz Waste, Pulp/Paper, and Air Matrices) Parameters are AOX/TOX, and
Dioxin/Furan. Method 1613 for Drinking Water.
State of Alabama, Department of Environmental Management. Expires December 31,
1997. Laboratory I.D. # 40950. Dioxin in drinking water.
State of Alaska, Department of Environmental Conservation. Expires December 21, 1997.
Certificate number OS-00397. Dioxin in drinking water.
State of Arizona, Department of Health Services. Expires May 26, 1998. Certificate
#A20423. Drinking Water for Dioxin, Dioxin in WW and S/H Waste.
State of Arkansas, Department of Pollution Control and Ecology. Expires February 18,
1998. Pulp/paper, soil, water, and Hazardous Waste for Dioxin/Furan; AOX/TOX.
State of California, Department of Health Services. Expires August 31, 1999. Certificate
#1922. Selected Metals in Waste Water, Volatiies, Semi-volatiles, and Dioxin/furan in WW and
Sol/Haz Waste. Dioxin in drinking water.
State of Connecticut, Department of Health Services. Recertification pending. Registration
# PH-0117. Dioxin in drinking water.
Delaware Health and Social Services. Expires December 31, 1997. Certificate #NC 140.
Dioxin in drinking water.
Florida Department of Health and Rehabilitative Services. Expires June 30, 1998.Dioxin in
DW. Drinking Water ID HRS# 87424. Metals, Extractable Organics (GC/MS), Pesticides/PCB's
(GC) and Volatiies (GC/MS) in Environmental Samples. Environmental water ID HRS#
ES7411.
Hawaii Department of Health. Expires March 1, 1998. Dioxin in drinking water. "Accepted"
status for regulatory purposes .
Rtvisad 10/28/97 RM
Pnnted 10/29/97 M< _ ul J"an9le Laboratories, Inc.
801 Caprtola Drive P.O. Box 13485
Durham, NC 27713-4411 Research Triangle Park, NC 27709-3485
919-544-5729 Fax #919-544-5491 _
O
-------
Idaho Department of Health and Welfare. Expires November 30, 1997. Dioxin in drinking
water.
State of Kansas, Department of Health and Environment Expires January 31, 1998.
Environmental Analyses/Non potable Water and Solid and Hazardous Waste. Method 1613
for drinking water. ID #s - Drinking water and/or pollution control - E-215. Solid or Hazardous
Waste-E-1209.
Commonwealth of Kentucky, Department for Environmental Protection. Expires
December 31, 1997. ID#90060. Dioxin in drinking water.
Maryland Department of Health and Mental Hygiene. Expires September 30, 1998.
Certification #235. Drinking water by Method 1613A.
State of Michigan, Department of Public Health. Expires June 3, 1998. Drinking water by
Method 1613.
Mississippi State Department of Health. No expiration date.. Dioxin in drinking water.
Montana Department of Health and Environmental Services. Expires December 31, 1997.
Dioxin in drinking water.
State of New Jersey, Department of Environmental Protection and Energy. Extended by
state. Temporary certificate until December 31, 1S97. ID #67851. BNAs and Volatiles. Dioxin in
drinking water.
State of New Mexico, Environment Department Recertification pending. Dioxin in drinking
water.
New York State Department of Health. Expires April 1, 1998. ID #11026. Environmental
Analyses of non-potable Water, Solid and Hazardous Waste. Method 1613 in DW.
State of North Carolina, Department of Environment Health and Natural Resources
Expires August 31, 1999. Certificate # 37751. Dioxin in drinking water.
State of North Carolina, Department of Environment, Health, and Natural Resources,
Division of Environmental Management Expires December 31, 1997. Certificate # 485.
Metals, pesticides & PCBs, semi-volatiles and volatfles; TCLP.
North Dakota State Department of Health and Consolidated Laboratories. Expires
December 31, 1997. Certificate # R-076. Effective October 4, 1993. Dioxin in drinking water.
Revised 10/28/97 RM
Printed 10/29/97
-------
Oklahoma Department of Environmental Quality. Expires August 31, 1998. Laboratory
#9612. Dioxin by 1613A, 8290 and 8280.
State of South Carolina, Department of Health and Environmental Control. Expires April 1,
1998. Certificate number #99040001 (drinking water). Expires August 31, 1999. Certificate
number #99040002 (other parameters). Dioxin/Furans, BNA, Volatiles, and RGBs/pesticides
under Clean Water Act, 2,3,7,8-TCDD for Drinking Water, and Organic extractables for Solid
and Hazardous Waste.
State of Tennessee. Department of Environment and Conservation. Expires February 5,
1999. ID #02992. Method 1613 Drinking water only.
U.S. Department of Agriculture Soil Permit Expires September 30, 2001. Permit No. S-
3790. Under the authority of the Federal Plant Pest Act, permission is granted to receive
foreign soil samples for use in laboratory analysis.
U.S. Army Corps of Engineers. Expires November 30, 1997. Validated to perform methods
8280 & 8290 for Lockboume Landfill Site Investigation, Defense Distribution Depot Projects,
and assorted projects for the USAGE North Pacific Division Laboratory.
U.S. EPA Region V. Expires November 14, 1999. Dioxin in drinking water.
U.S. EPA Region VIII, for the State of Wyoming. Expires November 13, 1997. Dioxin in
drinking water.
State of Utah, Department of Health. Expires December 31, 1997. Certificate Number E-166.
Certification for the following parameters: Semi-Volatiles and Volatiles under RCRA; Volatiles
under Clean Water Act; Dioxin/furans by Method 8280; Drinking water for Dioxin by Method
1613; Metals including Mercury and Microwave Digestion.
Commonwealth of Virginia, Department of General Services, Division of Consolidated
Laboratory Services. Expires June 30, 1998. ID # 00341. Dioxin in drinking water.
State of Washington, Department of Ecology. Expires September 11, 1998. Lab
Accreditation Number C067. Scope of Accreditation applies to water analyses for
Polychlorinated Dibenzo-p-dioxins and Polychlorinated Dibenzofurans, BNA Extr (Semivoiatile)
Organics and Purgeable (Volatile) Organics.
State of Washington, Department of Health. Expires April 30, 1998. Dioxin in drinking water
Lab I.D. 129
State of West Virginia, Department of Health. Expires December 31, 1997. Certificate No.
9923(C). Dioxin in drinking water.
10/28/97 RM
Printad 10/29/97
8
-------
State of Wisconsin, Department of Natural Resources. Expires August 31, 1998.
Laboratory ID Number 999869530. Certification for the following categories of Organics:
Purgeable, Base/Neutral, Acid, RGBs, and Dioxin. Expires November 14, 1999. Laboratory ID
999869530. Dioxin in drinking water.
PHARMACEUTICAL
Drug Enforcement Agency (DEA). Expires November 30, 1997. Registration number
RT01195835. Controlled substance registration for schedules 1,2,3,3N,4,5.
N.C. Department of Human Resources. Expires October 31, 1998. Registration number
NC-PT 0000 0031. North Carolina controlled substances registration. Application submitted for
renewal.
Food & Drug Administration (FDA) Registration. Expires June 1998. ID #3 001500
1053481. Annual registration of drug establishment Annual registration of drug establishment
OTHER
Clinical Laboratory Improvement Amendments (CUA) Registration. Expires May 30, 1999.
ID # 34D0705123. Department of Health & Human Services, Health Care Financing
Administration.
U.S. EPA Large Quantity Hazardous Waste Generator. No expiration date. EPA ID
#NCD982156879. Permit indicates that the laboratory is a large generator of hazardous waste.
North Carolina Radioactive Materials License. Expires April 30 1998. License No. 032-
0954-1. License authorizes the licensee to receive, acquire, own, possess, transfer, import and
use such radioactive materials as designated.
North Carolina General License for Radiation Protection. No. expiration date. License No.
032-875-OG. The general license applies only to radioactive material contained in devices
which have been manufactured and labeled in accordance with specific requirements.
R«viMd 10/28/97 RM
Printed 10/29/97
-------
ABBREVIATIONS
= BackHaif
CCB = Continuing Calibration Blank.
CCV =s Continuing Calibration Verification
CHECK HS * Check High Standard
D = DCP = Analytical Dupfrnte (Prepared Duplicate)
DA = Duplicate Analysis
FH = Front Half
FV =s Fnai Digestare Volume
ICB = Tp1*"9 I Calibration Blank
ICV = Tpirial Calibranon Verification
ICS AB = Interference Check Sohmon (Solution AB)
I = Tnirial
Solution AB contains common imerferents in addition to the analyte of interest.
IDL = Instrunant Detecnon Limit
L = Serial Dilution
LCS = Laboratory Control Spike Sample
\£B = Method Blank
MPV = Mercury Preparation Volume
MS = Pre-digestion Spike
MSD =s Pre-digestion Spike Duplicaie
N/A = Not Applicable
N/AV SB NOC AvaiTahte
N/V = Not Valid
PDS = Post-digestion Spike
%REC = Percent Recovery
RDL = Reporting Detection Thnir
RPD = Relative Percent Difference
T SB Analytical Triplicate (Prepared Triplicate; for Hg analysis by Method 7471 only)
TV = Total Sample Volume
< = Analyte concentration in the sample is less than the respective RDL
10
-------
STANDARD CONCENTRATIONS
for the TJA 61E TRACE ANALYZER
Analyte
Ag
As
-. -AT-"
B
Ba ?
Be
€a ^
Cd
- Ce ^'
ppb
ppb
ppb
ppb'.'.
ppb
ppb
ppb
ppbv
ppb
». '*
ppb*
ppb
High Std
'IflflOivS*
1000
<«>18fJ0Usi
1000
' v~tg@$;°«t
1000
• * - lOOOP^
1000
' ;;MJ':/:-
1000
10C»
1000
IiOOQj
10000
''">$Q0&-v-
1000
•"• 'lODO4?^
1000
10000
1000
1000
1000
1000
1000
rooo f
1000
1000- *
1000
- • -1000^^
1000
ICV/CCV
**?«: SOft- •'*'"'
500
4^1500^^
500
tr^SOO4^
500
,-^^seo-- '
500
r^:Soo-=
500
*' i 500
500
; 500
5000
H-: >%*$frf»
500
500000
500
' * '• '^•'^Mlffe^'^^
" '5^-3UwMF!'*
500
5000®D?
500
• -.^500.:-
500
- 500=
500
200000
19000
506 ;
500000
v-,50er- ;
500
'5000
500
500
500
506
500
- 500
650
; 500
500
",~500. -
500
RDL
> I ^
5
-.50. «
7
> 2 *
1
60 ^
1
3
1
2
2
40
220
'-- 1 '
30
' 2 '
2
300
3
30
2
4
3
13
1
8
5
2
12
Wavelength
3280
1890
*,:-:-"3esz^
2496
; ~;v-4934 •
3130
: 3179
2265
4186
2286
2677
3247
2714
7664
6706
2790
2576
2020
3302
2316
2149
2203
2068
1960
1899
4215
3349
1908
2924
2062
Note: Use this reference page to review the raw data from the TJA 6IE Trace Analyzer.
This page includes the standard concentrations for the check high standard, initial calibration
verification (ICV), continuing calibration verification (CCV), and the interference check solution
(ICSAB). In addition the reporting detection limit (RDL) and wavelength are reported for each
analyte.
Revision Date: 15-M-96
11
-------
CALCULATIONS FOR AIR SAMPLES
RESULTS FOR TRACE METALS (except mercury);
RESULT in jig (Front Half) = tig/L * FV rmL) * DF
1000 mL/L
. RESULT in u,g (Back Half & Impingers) = u.g/L * TV (mD * FV (mL) * DF
mL used * 1000 mL/L
FV = final volume in mL
TV = total volume in mL
DF = Dilution Factor
The RESULTS for combined Front Half & Back Half samples use the same calculation as the
Back Half & impinger samples.
RESULTS FOR MERCURY fHg):
RESULT in jig (Front Half) = |ig/L * (mL FV/mL aliquot) * MPV * DF
RESULT in U-g (Back Half & Impingers) = (ig/L * (mL TV/mL aliquot) * MPV * DF
MPV = mercury preparation volume = 0.1 L
%REC (Percent Recovery) for MS/MSP He spikes:
%REC = spike sample results - original sample results * 100
true spike sample results
NOTE: Original sample results less than the RDL are not used in calulations.
%REC (Percent Recovery) for PDS:
%REC = Spike sample iig/L cone. - original sample \isfL cone. * 100
spike cone. (jig/L)
%REC (Percent Recovery) for LCS/LCSD:
%REC = Spike sample |ig/L cone. * 100
spike cone. Qig/L)
RPDs: RPD *' I Result 2 - Result 1 I * 100
(Result 2 + Result l)/2 Rev. 2-Oct-96
12
-------
Client: Pacific Environmental Services
Project Number: 43377
Sample Report
Client Sample ID:
TLI Sample ID-
Date Received'
Date Prepared:
Date Analyzed'
Matrix:
0-M29-1-FHACEJHAR.FILTER FH
184-50-1ABC FH
September 24. 1997
October 10-14. 1997
October 16.20.21 & 22. 1997
Air
Aftstyte "
Aa
As
Ba
Be
Cd
Co
Cr
Cu
Mn
Ni
P
Pb
Sb
Se
Tl
Zn
Oona
ftnU
-0.509
26.614
2210.242
-9.136
2.179
18.249
147.007
173.186
2033.351
72.575
3317.880
197.328
44.560
43.871
1.400
1144.375
BC ' :
TdalVol
N/A
N/A
N/A
N/A
N/A
N/A
N/A
N/A
N/A
N/A
N/A
N/A
N/A
N/A
N/A
N/A
Hi
Used
N/A
N/A
N/A
N/A
N/A
N/A
N/A
N/A
N/A
N/A
N/A
N/A
N/A
N/A
N/A
N/A
*t
Final Vo!
100
100
100
100
100
100
100
100
100
100
100
100
100
100
100
100
„ ailulbn
Victor '
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
tctaJ«$
Rest*
< 0.1
2.66
221
< 0.100
0.218
1.820
14.7
17.3
203
7.26
332
19.7
4.46
4.39
< 0.200
114
Triangle Laboratories, Inc.
801 Capitola Drive * Durham, North Carolina 27713
Tele: (919) 544-5729 * Fax: (919) 544-5491
Printed: 03-Nov-97 at 01:08PM
13
-------
Client: Pacific Environmental Services
Project Number: 43377
Sample Report
Client Sample D>
TLI Sample ID-
Date Received:
Date Prepared:
Date Analyzed:
Matrix:
O-M29-1-FHACE.FHAR.FILTER FH L
184-50-1ABC FH L
September 24, 1997
October 10-14, 1997
October 16.20.21 & 22. 1997
Air
Asalvte
Aq
As
Ba
Be
Cd
Co
Cr
Cu
Mn
Ni
P
Pb
Sb
Se
Tl
Zn
Cow?/
&
-------
Client: Pacific Environmental Services
PrQJect Number: 43377
Sample Report
Client Sample ID:
TLI Sample ID:
Date Received:
Date Prepared:
Date Analyzed'
Matrix:
O-M29-1-HNO3 BH
184-50-1DBH
Seotember24. 1997
October 10-14. 1997
October 16.20.21 & 22. 1997
Air
Analvte :
Aa
As
Ba
Be
Cd
Co
Cr
Cu
Mn
Ni
P
Pb
Sb
Se
Tl
Zn
Cona
{MM
0.277
-2.638
20.506
-0.125
5.845
-2.288
11.391
22.134
45.093
16.338
620.845
63.809
3.419
5.132
-0.50
280.848
^*
fat
Toiafvor;
954
954
954
954
954
954
954
954
954
954
954
954
954
954
954
954
s rrl
*'U«f s
854
854
854
854
854
854
854
854
854
854
854
854
854
854
854
854
at ,
RrerfVoL1
100
100
100
100
100
100
100
100
100
100
100
100
100
100
100
100
Diution
Factor
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
I fotelua i
Result ;
< 0.112
< 0.559
229
< 0.112
0.653
< 0.112
1.27
2.47
5.04
1.83
69.4
7.13
< 0.447
0.573
< 0.223
31.4
Triangle Laboratories, Inc.
801 Capitola Drive * Durham, North Carolina 27713
Tele: (919) 544-5729 * Fax: (919) 544-5491
Printed: 03-Nov-97 at 01:08 PM
-------
Client: Pacific Environmental Services
Project Number: 43377
Sample Report
Client Sample ID:
TLI Sample ID-
Date Received:
Date Prepared:
Date Analyzed'
Matrix:
O-M29-1-HNO3 BH L
184-50-1DBHL
September 24. 1997
October 10-14. 1997
October 16.20.21 & 22. 1997
Air
j.
Analvte i
Aa
As
Ba
Be
Cd
Co
Cr
Cu
Mn
Ni
P
Pb
Sb
Se
Tl
Zn
Gooc,
footo
-0.090
-1.821
2.332
-0.050
1.419
-0.174
1.220
3.320
4.133
2.951
131.717
12.379
-0.995
1.379
-0.90
58.600
• rat
Total Vof:
954
954
954
954
954
954
954
954
954
954
954
954
954
954
954
954
nt.
Used
854
854
854
854
854
854
854
854
854
854
854
854
854
854
854
854
nt
RnatVbL
100
100
100
100
100
100
100
100
100
100
100
100
100
100
100
100
Dilution
fSt&Qf
5
5
5
5
5
5
5
5
5
5
5
5
5
5
5
5
TotaJug i
Result
< 0.559
< 2.79
1.30
< 0.559
0.793
< 0.559
< 1.12
1.85
2.31
< 1.68
73.6
6.91
< 223
< 1.68
< 1.12
32.7
Triangle Laboratories, Inc.
801 Capitola Drive * Durham, North Carolina 27713
Tele: (919) 544-5729 * Fax: (919) 544-5491
Printed: 03-Nov-97 at OL08PM
16
-------
Client: Pacific Environmental Services
Project Number: 43377
Sample Report
Client Sample ID:
TLI Samole ID:
Date Received:
Date Prepared:
Date Analyzed:
Matrix:
O-M29-2-FHACE JHAR.FILTER FH
184-50-2ABCFH
September 24. 1997
October 10-14. 1997
October 16.20.21 & 22. 1997
Air
Anah/te \
Aa
As
Ba
Be
Cd
Co
Cr
Cu
Mn
Ni
P
Pb
Sb
Se
TI
Zn
Gooa
totfti
1.729
5.922
510.774
-1.516
21.333
-18.808
99.655
44.251
333.693
60.858
603.530
57.817
41.463
39.586
2.100
466.631
BiL A^A>;
Total Vbtf/J
N/A
N/A
N/A
N/A
N/A
N/A
N/A
N/A
N/A
N/A
N/A
N/A
N/A
N/A
N/A
N/A
* * rat V
^Used
N/A
N/A
N/A
N/A
N/A
N/A
N/A
N/A
N/A
N/A
N/A
N/A
N/A
N/A
N/A
N/A
, r"»i ,:
FhafVof.
100
100
100
100
100
100
100
100
100
100
100
100
100
100
100
100
.Ofcfcn -
Factor
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
sj<$3tm
- " Rest*
0.173
0.592
51.1
< 0.100
2.13
< 0.1
9.97
4.43
33.4
6.09
60.4
5.78
4.15
3.96
0.210
46.7
Triangle Laboratories, Inc.
801 Capitola Drive * Durham, North Carolina 27713
Tele: (919) 544-5729 * Fax: (919) 544-5491
Printed: 03-Nov-97 at 01:08PM
17
-------
Client: Pacific Environmental Services
Project Number: 43377
Sample Report
Client Sample ID:
TLI Sample ID-
Date Received'
Date Prepared:
Date Analvzed:
Matrix:
O-M29-2-FHACE J^HARFILTER FH DA
184-50-2ABCFHDA
September 24. 1997
October 10-14. 1997
October 16.20.21 & 22. 1997
Air
Analyte i
Aa
As
Ba
Be
Cd
Co
Cr
Cu
Mn
Ni
P
Pb
Sb
Se
Tl
Zn
Gone,
fciofU
1.879
9.131
508.461
-1.543
21.142
-19.059
100.776
43.699
333.777
61.462
595.276
55.996
42.580
40.579
N/A
467.375
,
rot :
TciaiVa^
N/A
N/A
N/A
N/A
N/A
N/A
N/A
N/A
N/A
N/A
N/A
N/A
N/A
N/A
N/A
N/A
rat ,
• Used
N/A
N/A
N/A
N/A
N/A
N/A
N/A
N/A
N/A
N/A
N/A
N/A
N/A
N/A
N/A
N/A
**fc ,,,;
Final Vd. :
100
100
100
100
100
100
100
100
100
100
100
100
100
100
N/A
100
Dilution
Factor
1
1
1
1
1
1
1
1
1
1
1
1
1
1
N/A
1
TotaJug
> Rest*
0.188
0.913
50.8
< 0.100
2.11
< 0.100
10.1
4.37
33.4
6.15
59.5
5.60
4.26
4.06
N/A
46.7
Triangle Laboratories, Inc.
801 Capitola Drive * Durham, North Carolina 27713
Tele: (919) 544-5729 * Fax: (919) 544-5491
Printed: 03-Nov-97 at 01:08PM
18
-------
Client: Pacific Environmental Services
Project Number; 43377
Sample Report
Client Sample ID:
TLI Saruole ID'
Date tteceived:
Date Prepared:
Date Analyzed'
Matrix: .
0-M29-2-HNO3 BH
184-50-2DE BH
Sentember24. 1997
October 10-14. 1997
October 16.20.21 & 22. 1997
Air
Anslyte
Aa
As
Ba
Be
Cd
Co
Cr
Cu
Mn
Ni
P
Pb
Sb
Se
Tl
Zn
.Cfcna
ft***
0.568
-7.156
8.581
-0.007
0.848
-1.476
4.083
19.038
15.930
7.948
547.642
23.644
0.771
3.153
-0.10
146.490
.. FflL
TdalVoL
1645
1645
1645
1645
1645
1645
1645
1645
1645
1645
1645
1645
1645
1645
1645
1645
- ftiL
- Used
1545
1545
1545
1545
1545
1545
1545
1545
1545
1545
1545
1545
1545
1545
1545
1545
at
RnaJVd.
100
100
100
100
100
100
100
100
100
100
100
100
100
100
100
100
Dilution
tractor
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
Total ws i
Ttesyft
< 0.106
< 0.532
0.914
< 0.106
< 0.106
< 0.106
0.435
2.03
1.70
0.846
58.3
2.52
< 0.426
0.336
< 0.213
15.6
Triangle Laboratories, Inc.
801 Capitola Drive * Durham, North Carolina 27713
Tele: (919) 544-5729 * Fax: (919) 544-5491
Printed: 03-Nov-97 at 01:08 PM
19
-------
Client: Pacific Environmental Services
Project Number; 43377
Sample Report
Client Sample ID:
TLI Sample ID-
Date Received:
Date Preoared:
Date Analvzed4
Matrix:
O-M29-HNO3BHDA
184-50-2DE BH DA
September 24. 1997
October 10-14. 1997
October 16.20.21 & 22. 1997
Air
Aralvte
Aa
As
Ba
Be
Cd
Co
Cr
Cu
Mn
Ni
P
Pb
Sb
Se
Tl
Zn
Oone>
&0?U
-0.003
-8.639
8.590
-0.054
1.010
-1.200
4.012
18.268
16.004
8.008
541.735
23.731
1.277
1.535
N/A
147.369
0*.
TofetfVol
1645
1645
1645
1645
1645
1645
1645
1645
1645
1645
1645
1645
1645
1645
N/A
1645
nt "
Used
1545
1545
1545
1545
1545
1545
1545
1545
1545
1545
1545
1545
1545
1545
N/A
1545
Hi
RradVd.
100
100
100
100
100
100
100
100
100
100
100
100
100
100
N/A
100
Dilution
Factor
1
1
1
1
1
1
1
1
1
1
1
1
1
1
N/A
1
ToteP«g ;
Result ;
< 0.106
< 0.532
0.915
< 0.106
0.108
< 0.106
0.427
1.94
1.70
0.853
57.7
2.53
< 0.426
< 0.319
N/A
15.7
Triangle Laboratories, Inc.
801 Capitola Drive * Durham, North Carolina 27713
Tele: (919) 544-5729 * Fax: (919) 544-5491
Printed: 03-Nov-97 at 01:08PM
20
-------
Client: Pacific Environmental Services
Project Number: 43377
Sample Report
Client Sample ID:
TLI Sample ID:
Date Received:
Date Prepared:
Date Analyzed:
Matrix:
O-M29-3-FHACE JHAR.FDLTER FH
184-50-3ABC FH
September 24. 1997
October 10-14. 1997
October 16.20.21 & 22. 1997
Air
BSfivti
Aq
As
Ba
Be
Cd
Co
Cr
Cu
Mn
Ni
D
Pb
Sb
Se
Tl
Zn
Cone.
totfti
8.915
7.679
213.783
-0.601
-0.976
-15.077
78.480
32.218
142.085
43.197
258.320
31.038
33.494
30.059
2.30
202.846
mL
TctalVoi
N/A
N/A
N/A
N/A
N/A
N/A
N/A
N/A
N/A
N/A
N/A
N/A
N/A
N/A
N/A
N/A
: ftt
Used
N/A
N/A
N/A
N/A
N/A
N/A
N/A
N/A
N/A
N/A
N/A
N/A
N/A
N/A
N/A
N/A
ml,
FfnafVal
100
100
100
100
100
100
100
100
100
100
100
100
100
100
100
100
Dilution
Factor ,
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
Total «s
Resuft
0.892
0.768
21.4
< 0.100
< 0.100
< 0.100
7.85
3.22
14.2
4.32
25.8
3.10
3.35
3.01
0.230
20.3
Triangle Laboratories, Inc.
801 Capitola Drive * Durham, North Carolina 27713
Tele: (919) 544-5729 * Fax: (919) 544-5491
Printed: 03-Nov-97 at 01:08PM
21
-------
Client: Pacific Environmental Services
Project Number: 43377
Sample Report
Client Sample ED:
TLI Sample ID-
Date Received:
Date Prepared:
Date Analyzed'
Matrix:
O-M29-3-HNO3 BH
184-50-3DE BH
September 24. 1997
October 10-14. 1997
October 16.20.21 & 22. 1997
Air
Analvte
Aa
As
Ba
Be
Cd
Co
Cr
Cu
Mn
Ni
P
Pb
Sb
Se
Tl
Zn
Cone.
ft***
0.191
-7.223
11.257
-0.054
16.442
-0.577
6.680
52.085
17.223
34.806
747.814
964.422
-0.531
86.488
1.50
192.074
, ^rsL
TotaiVol
1130
1130
1130
1130
1130
1130
1130
1130
1130
1130
1130
1130
1130
1130
1130
1130
friL
Used
1030
1030
1030
1030
1030
1030
1030
1030
1030
1030
1030
1030
1030
1030
1030
1030
Rt
RnalVal.
100
100
100
100
100
100
100
100
100
100
100
100
100
100
100
100
DiutJor.
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
totetftjsi
Result
< 0.110
< 0.549
1.23
< 0.110
1.80
< 0.110
0.733
5.71
1.89
3.82
82.0
106
< 0.439
9.49
< 0.219
21.1
Triangle Laboratories, Inc.
801 Capitola Drive * Durham, North Carolina 27713
Tele: (919) 544-5729 * Fax: (919) 544-5491
Printed: 03-Nov-97 at 01:08 PM
22
-------
Client: Pacific Environmental Services
Project Number: 43377
Sample Report
Client Sample ID:
TLI Sample ID:
Date Received:
Date Prepared:
Date Analyzed'
Matrix:
O-M294-FHACaFHAR,FILTER FH
184-50-4ABC FH
September 24. 1997
October 10-14. 1997
October 16.20.21 & 22. 1997
Air
Aaalvte \
Aa
As
Ba
Be
Cd
Co
Cr
Cu
Mn
Ni
P
Pb
Sb
Se
Tl
Zn
Oona -
fcioto
2.082
4.111
139.273
-0.365
-2.418
-16.291
64.361
21.367
204.413
28.942
142.275
6.657
27.323
24.357
-1.00
160.507
- ',-nt. ,
' TV&Vtit
N/A
N/A
N/A
N/A
N/A
N/A
N/A
N/A
N/A
N/A
N/A
N/A
N/A
N/A
N/A
WA
- si
Used '
N/A
N/A
N/A
N/A
N/A
N/A
N/A
N/A
N/A
N/A
N/A
N/A
N/A
N/A
N/A
N/A
Hi -
FfnsflVoJ.
100
100
100
100
100
100
100
100
100
100
100
100
100
100
100
100
-, Otaifcr
' Factor '
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
Total us
Resuft
0208
< 0.500
13.9
< 0.100
< 0.100
< 0.100
6.44
2.14
20.4
2.89
14.2
0.666
2.73
2.44
< 0.200
16.1
Triangle Laboratories, Inc.
801 Capitola Drive * Durham, North Carolina 27713
Tele: (919) 544-5729 * Fax: (919) 544-5491
Printed: 03-Nov-97 at 01:08PM
23
-------
Client: Pacific Environmental Services
Project Number: 43377
Sample Report
Client Sample ID:
TLI Sample ID-
Date Received'
Date Prepared:
Date Analvzed'
Matrix:
O-M29^-HNO3 BH
184-50-4DE BH
September 24. 1997
October 10-14. 1997
October 16.20.21 & 22. 1997
Air
Analvte i
Aa
As
Ba
Be
Cd
Co
Cr
Cu
Mn
Ni
P
Pb
Sb
Se
Tl
Zn
COOfc
footo
0.311
-6.866
5.349
-0.016
0.131
-1.7BO
2.399
11.289
491.453
8.884
555.480
12.479
-1.163
0.932
0.80
94.302
s
mL *,
Total VoT
1105
1105
1105
1105
1105
1105
1105
1105
1105
1105
1105
1105
1105
1105
1105
1105
'' JtiL
Used
1005
1005
1005
1005
1005
1005
1005
1005
1005
1005
1005
1005
1005
1005
1005
1005
aL
Rraavol.
100
100
100
100
100
100
100
100
100
100
100
100
100
100
100
100
DUutJon;
"'lector
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
Totefug
Result
< 0.110
< 0.550
0.588
< 0.110
< 0.110
< 0.110
0264
1.24
54.0
0.977
61.1
1.37
< 0.440
< 0.330
< 0.220
10.4
Triangle Laboratories, Inc.
801 Capitola Drive * Durham, North Carolina 27713
Tele: (919) 544-5729 * Fax: (919) 544-5491
Printed: 03-Nov-97 at 01:08PM
24
-------
Client: Pacific Environmental Services
Project Number: 43377
Sample Report
Client Sample ID:
TLI Sample ID:
Date Received'
Date Prepared'
Date Analyzed:
Matrix'
0-M29-FB-FHACE JHAR.FILTER FH
184-50-5 ABC FH
Sentember24. 1997
October 10-14. 1997
October 16.20.21 & 22. 1997
Air
Anah/te \
Aq
As
Ba
Be
Cd
Co
Cr
Cu
Mn
Ni
P
Pb
Sb
Se
TI
Zn
Cona
ft«to
1.066
6.275
46.626
-0.052
-6.656
-31.577
94.985
10.522
10.861
48.171
0.201
-20.784
49.090
42.696
1.20
30.196
R*. ,:
TetalVal
N/A
N/A
N/A
N/A
N/A
N/A
N/A
N/A
N/A
N/A
N/A
N/A
N/A
N/A
N/A
N/A
' *dL *
Used
N/A
N/A
N/A
N/A
N/A
N/A
N/A
N/A
N/A
N/A
N/A
N/A
N/A
N/A
N/A
N/A
SiL' ' :
Final Vol.
100
100
100
100
100
100
100
100
100
100
100
100
100
100
100
100
Oilution
Factor
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
Tofedws
Reset
0.107
0.627
- 4.66
< 0.100
< 0.100
< 0.100
9.50
1.05
1.09
4.82
< 3.00
< 0.200
4.91
427
< 0.200
3.02
Triangle Laboratories, Inc.
801 Capitola Drive * Durham, North Carolina 27713
Tele: (919) 544-5729 * Fax: (919) 544-5491
Printed: 03-Nov-97 at 01:08PM
-------
Client: Pacific Environmental Services
Project Number: 43377
Sample Report
Client Sample ID:
TLI Sample ID:
Date Received:
Date Prepared:
Date Analvzed'
Matrix:
O-M29-FB-HNO3 BH
184-50-5BD BH
September 24. 1997
October 10-14. 1997
October 16.20.21 & 22. 1997
Air
Analyte \
Aa
As
Ba
Be
Cd
Co
Cr
Cu
Mn
Ni
P
Pb
Sb
Se
Tl
Zn
Cfcne.
ftioU
-0.084
-5.436
2.368
-0.037
1.295
-0.835
3.764
6.244
71.682
2.070
120.688
65.879
0.971
4.210
-2.80
29.576
.*
rat
TotalVoL I
150
150
150
150
150
150
150
150
150
150
150
150
150
150
150
150
v ni.
Used
150
150
150
150
150
150
150
150
150
150
150
150
150
150
150
150
-'8i -'' >-
FinaJVd.
100
100
100
100
100
100
100
100
100
100
100
100
100
100
100
100
5 D&rtfc>r» i
Factor
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
TotaJus
Result "
< 0.100
< 0.500
0.237
< 0.100
0.130
< 0.100
0.376
0.624
7.17
< 0.300
12.1
6.59
< 0.400
0.421
< 0.200
2.96
Triangle Laboratories, Inc.
801 Capitola Drive * Durham, North Carolina 27713
Tele: (919) 544-5729 * Fax: (919) 544-5491
Printed: 03-Nov-97 at 01:08PM
26
-------
Client: Pacific Environmental Services
Project Number: 43377
Sample Report
Client Sample ID:
TLI Sample D>
Date Received:
Date Prepared:
Date Analyzed'
Matrix:
O-M29-RB-FHACE.FHARJTLTER FH
184-50-6ABC FH
September 24. 1997
October 10-14. 1997
October 16.20.21 & 22. 1997
Air
Analyte •
Aq
As
Ba
Be
Cd
Co
Cr
Cu
Mn
Ni
P
Pb
Sb
Se
Tl
Zn
Cotva
.fcoto. -
2.705
3.407
43.292
-0.112
-6.215
-29.571
93.294
10.580
9.109
46.803
17.600
-12.883
41.765
43.531
-3.00
25.989
.*
Hi - . j
TctelVdl *
N/A
N/A
N/A
N/A
N/A
N/A
N/A
N/A
N/A
N/A
N/A
N/A
N/A
N/A
N/A
N/A
ral - -
" Used -
N/A
N/A
N/A
N/A
N/A
N/A
N/A
N/A
N/A
N/A
N/A
N/A
N/A
N/A
N/A
N/A
111
Final V&L
100
100
100
100
100
100
100
100
100
100
100
100
100
100
100
100
Dillon
Factor *
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
* fotaiu®
Resuft
0.270
< 0.500
4.33
< 0.100
< 0.100
< 0.100
9.33
1.06
0.911
4.68
< 3.00
< 0.200
4.18
4.35
< 0.200
2.60
Triangle Laboratories, Inc.
801 Capitola Drive * Durham, North Carolina 27713
Tele: (919) 544-5729 * Fax: (919) 544-5491
Printed: 03-Nov-97 at 01:08PM
27
-------
Client: Pacific Environmental Services
Project Number: 43377
Sample Report
Client Sample ID:
TLI Samole ID:
Date Received'
Date Prepared:
Date Analvzed:
Matrix:
O-M29-RB-HNO3 BH
184-50-6BD BH
September 24. 1997
October 10-14. 1997
October 16.20.21 & 22. 1997
Air
Anah/te
Aa
As
Ba
Be
Cd
Co
Cr
Cu
Mn
Ni
P
Pb
Sb
Se
Tl
Zn
Cona
luato
0.061
-8.994
3.256
-0.044
-0.536
-1.619
2.217
14.381
346.891
6.056
553.359
2.647
1.642
-0.017
-1.50
20.330
-
' iat
TotalVof,
300
300
300
300
300
300
300
300
300
300
300
300
300
300
300
300
frt.
Used
300
300
300
300
300
300
300
300
300
300
300
300
300
300
300
300
Ri *
Final Vo!.
100
100
100
100
100
100
100
100
100
100
100
100
100
100
100
100
m&x*''
Factor :
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
!' $Qiof*8i
Result
< 0.100
< 0.500
0.326
< 0.100
< 0.100
< 0.100
0999
1.44
34.7
0.606
55.3
0.265
< 0.400
< 0.300
< 0.200
2.03
Triangle Laboratories, Inc.
801 Capitola Drive * Durham, North Carolina 27713
Tele: (919) 544-5729 * Fax: (919) 544-5491
Printed: 03-Nov-97 at 01:08PM
23
-------
Client: Pacific Environmental Services
Project Number; 43377
Sample Report
Client Sample ID:
TLI Sample ID:
Date Received:
Date Prepared:
Date Analyzed:
Matrix:
I-M29- 1-FHACE.FHARJTLTER FH
184-50-7 ABC FH
September 24. 1997
October 10-14. 1997
October 16.20.21 & 22. 1997
Air
Analvt&
Aq
As
Ba
Be
Cd
Co
Cr
Cu
Mn
Ni
P
Pb
Sb
Se
TI
Zn
Gorxv
fcertX
-15.487
152.097
6171.882
-35.757
60.007
265.325
358.682
1251.144
11640.313
160.800
34933.355
450.776
-2.294
-55.967
29.038
5032.940
, ~#r$*,<.
IttoW* <:
N/A
N/A
N/A
N/A
N/A
N/A
N/A
N/A
N/A
N/A
N/A
N/A
N/A
N/A
N/A
N/A
^'XfBl *
'"""ttead
N/A
N/A
N/A
N/A
N/A
N/A
N/A
N/A
N/A
N/A
N/A
N/A
N/A
N/A
N/A
N/A
SlLX :
FitetfVst
100
100
100
100
100
100
100
100
100
100
100
100
100
100
100
100
Dilution
'factor"
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
-T<*aJ«g,
Best*:
< 0.100
15.2
617
< 0.100
6.00
26.5
35.9
125
1160
16.1
3490
45.1
< 0.400
< 0.300
2.90
503
Triangle Laboratories, Inc.
801 Capitola Drive * Durham, North Carolina 27713
Tele: (919) 544-5729 * Fax: (919) 544-5491
Printed: 03-Nov-97 at 01:08PM
29
-------
Client: Pacific Environmental Services
Project Number: 43377
Sample Report
Client Sample ID:
TLI Sample ID:
Date Received'
Date Prepared:
Date Analyzed:
Matrix:
I-M29-1-HNO3 BH
184-50-7D BH
September 24. 1997
October 10-14, 1997
October 16.20.21 & 22. 1997
Air
Analvte I
Aa
As
Ba
Be
Cd
Co
Cr
Cu
Mn
Ni
P
Pb
Sb
Se
Tl
Zn
Qwxx
&9to
0.376
-2.937
4.655
-0.012
5.279
-1.085
6.758
7.221
109.380
7.742
447.197
42.647
-0.046
7.465
0.40
163.332
FflL v
TotalVof.
435
435
435
435
435
435
435
435
435
435
435
435
435
435
435
435
" rtL :
" Used
335
335
335
335
335
335
335
335
335
335
335
335
335
335
335
335
at ;!
Rna5Vd.
100
100
100
100
100
100
100
100
100
100
100
100
100
100
100
100
D&iforj :
Factor
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
Tofefwg
< Result
< 0.130
< 0.649
0.604
< 0.130
0.686
< 0.130
0.878
0.938
14.2
1.01
58.1
5.54
< 0.519
0.969
< 0.26
21.2
Triangle Laboratories, Inc.
801 Capitola Drive * Durham, North Carolina 27713
Tele: (919) 544-5729 * Fax: (919) 544-5491
Printed: 03-Nov-97 at 01:08 PM
30
-------
Client: Pacific Environmental Services
Protect Number: 43377
QA: Serial Dilution
Client Sanrole ID:
TLI Sample ID:
Date Prepared:
Date Analyzed'
Matrix:
O-M29-1-FHACEJ7HAR.FILTER FH
184-50-1ABCFH
October 10-14. 1997
October 16.20.21 & 22. 1997
Air
O-M29-1-FHAGELFHAR.FILTER FH L
184-50-1ABCFHL
October 10-14. 1997
October 16.20 21 & 22. 1997
Air
AfjaMe
Aq
As
Ba
Be
Cd
Co
Cr
Cu
Mn
Ni
P
Pb
Sb
Se
TI
Zn
Native Sample
- isTkaiqBo**"!
** vat* *m
< 0.100
2.66
221
< 0.100
0.218
1.82
14.7
17.3
203
7.26
332
19.7
4.46
4.39
< 0.200
114
"«"
Gains*.".
-0.509
26.614
2210.242
-9.136
2.179
18.249
147.007
173.186
2033.351
72.575
3317.880
197.328
44.560
43.871
1.400
1144.375
Serial Dilution
---<;' , , 1 'T<3taJ «f^^
< 0.500
< 2.50
242
< 0.500
< 0.500
1.95
18.2
18.1
226
8.72
385
23.0
4.91
5.40
N/A
130
%."&&, *w
$• /?', ~tt """-
-'-'- xOj0a
-0.444
3.164
484.810
-1.931
0.372
3.906
36.485
36.293
451.437
17.447
769.575
45.976
9.814
10.801
N/A
260.071
V;. fv.
""••1RR3
-------
Client: Pacific Environmental Services
Project Number: 43377
QA: Serial Dilution
Client Sample ID:
TLI Sample ID:
Date Preoared:
Date Analyzed'
Matrix:
O-M29-1-HNO3 BH
184-50-1D BH
October 10-14. 1997
October 16 20.21 & 22. 1997
Air
O-M29-1-HNO3RHI,
184-50-1DBHL
October 10-14. 1997
October 16.20.21 & 22. 1997
Air
Analyte
Aq
As
Ba
Be
Cd
Co
Cr
Cu
Mn
Ni
P
Pb
Sb
Se
Tl
Zn
Native Sample
1fctef.«9 ! J
$0Sldt " " "I
< 0.112
< 0.559
2.29
< 0.112
0.653
< 0.112
1.27
2.47
5.04
1.83
69.4
7.13
< 0.447
0.573
< 0.223
31.4
- i#L
Cone.
0.277
-2.638
20.506
-0.125
5.845
-2.288
11.391
22.134
45.093
16.338
620.845
63.809
3.419
5.132
-0.500
280.848
Serial Dilution
- TaiaiuS'- -
-------
Client: Pacific Environmental Services
Project Number: 43377
QA: Duplicate
Client Sample ID:
TLI Samole ID:
Date Prepared'
Date Analyzed:
Matrix:
O-M29-2-FHACE.FHAR.FILTER FH
184-50-2ABC FH
October 10-14. 1997
October 16.20.21 & 22. 1997
Air
O-M29-2-FHACRFHARJTLTER FH DA
184-50-2ABCFHDA
October 10-14 1997
Oaober 16.20.21 & 22. 1997
Air
Arafyte
Aa
As
Ba
Be
Cd
Co
Cr
Cu
Mn
Ni
P
Pb
Sb
Se
Tl
Zn
Sample
Tots* 09
Result
0173
0.592
51.1
< 0.100
2.13
< 0.100
9.97
4.43
33.4
6.09
60.4
5.78
4.15
3.96
0.210
46.7
s ' «$L
'Cowi
1.729
5.922
510.774
-1.516
21.333
-18.808
99.655
44.251
333.693
60.858
603.530
57.817
41.463
39.586
2.100
466.631
Duplicate
- * Tefelag " *s '
<> 8as&.< ': \
0188
0.913
50.8
< 0.100
2.11
< 0.100
10.1
4.37
33.4
6.15
59.5
5.60
4.26
4.06
N/A
46.7
*/ -m
' ••>C0fJ& >
1 879
9.131
508.461
-1.543
21.142
-19.059
100.776
43.699
333.777
61.462
595.276
55.996
42.580
40.579
N/A
467.375
RPQ
-------
Client: Pacific Environmental Services
Project Number: 43377
QA: Duplicate
Client Sample ID-
TLI Sample ID-
Date Prepared-
Date Analyzed"
Matrix:
O-M29-2-HNO3 BH
184-50-2DE BH
October 10-14. 1997
October 16.20.21 & 22. 1997
Air
O-M29-HNO3 BH DA
184-50-2DEBHDA
October 10-14. 1997
October 16.20.21 & 22. 1997
Air
Anahrte
Aq
As
Ba
Be
Cd
Co
Cr
Cu
Mn
Ni
P
Pb
Sb
Se
Tl
Zn
Sample
" Totelug I
Result i
< 0.106
< 0.532
0.914
< 0.106
< 0.106
< 0.106
0.435
2.03
1.70
0.846
58.3
2.52
< 0.426
0.336
< 0.213
15.6
•
,J4Jj!t *"
Conn"
0.568
-7.156
8.581
-0.007
0.848
-1.476
4.083
19.038
15.930
7.948
547.642
23.644
0.771
3.153
-0.100
146.490
Duplicate
^ - -.. ,^fc*ah£ ;-;
' ftesuS -» "
< 0.106
< 0.532
0.915
< 0.106
0.108
< 0.106
0.427
1.94
1.70
0.853
57.7
2.53
< 0.426
< 0.319
N/A
157
*,**,*&('' ''
" Cflnft
-0.003
-8.639
8.590
-0.054
1.010
-1.200
4.012
18.268
16.004
8.008
541.735
23.731
1.277
1.535
N/A
147.369
v ,?-.>
"HPD
', >
-------
Client: Pacific Environmental Services
Project Number; 43377
QA: Matrix Spikes (Post-Digestion)
Client Samole H>
TLI Sample ID:
Date Prepared:
Date Analw.ert:
Matrix:
OM29-1-FHACE.FHAR.RLTER FH PDS
184-50-1ABCFHPDS
October 10-14, 1997
October 16.20.21 & 22. 1997
Air
-AnaMs i
Aa
As
Ba
Be
Cd
Co
Cr
Cu
Mn
Ni
P
Pb
Sb
Se
Tl
Zn
Post-Dig
•.Rsewepecf 2
Amounf&itjfl.}
37.13
66.21
220764
31.50
44.31
60.73
187.14
216.04
2026.71
112.31
4053.51
231.32
83.39
80.62
N/A
1289.01
estion Spike
,' '•<>••* •> f ^Srlik& * ^ ^ -.0^^
- -"" AxmwA{..
...
...
—
„
...
...
—
...
—
—
...
...
...
...
...
—
...
—
...
.
—
„_
«-
...
...
Triangle Laboratories, Inc.
801 Capitola Drive * Durham, NC 27713
Tele: (919) 544-5729 * Fax: (919) 544-5491
Printed: 03-Nov-97
at
02:17PM
-------
Client: Pacific Environmental Services
Project Number: 43377
QA: Matrix Spikes (Post-Digestion)
Client Samole ID:
TLI Samole ID:
Date Prepared:
Date Analyzed:
Matrix:
O-M29-1-HNO3BHPDS
184-50- ID BHPDS
October 10-14, 1997
October 16.20.21 & 22, 1997
Air
AnaiVte
Aa
As
Ba
Be
Cd
Co
Cr
Cu
Mn
Ni
P
Pb
Sb
Se
TI
Zn
Post-Diqestion Spike
Recovered
Amount ftjoiO
41.57
36.64
60.46
45.63
52.79
46.23
55.26
69.47
68.47
61.19
1409.02
108.50
47.69
46.09
20.6
456.69
/ 'Sp&, ' :
'tim^'tv&ti
50
50
50
50
50
50
50
50
50
50
1000
50
50
50
25
200
*«•**"
Recovsiv
83°/c
73%
80%
91%
94%
92°/<
88%
95°/c
47%
90°/c
79%
89%
95%
82%
82%
88%
Post-Diqestion Spike Duplicate
&eo^retts,
Amburitfao/b
, &**,
Amount foo/U
,- « 1
^Recoveiv^
^ BPD,.
—
—
—
—
—
—
—
—
—
—
—
—
—
—
—
—
—
—
—
—
—
—
—
—
—
_.
—
—
—
—
—
Triangle Laboratories, Inc.
801 Capitola Drive * Durham, NC 27713
Tele: (919) 544-5729 * Fax: (919) 544-5491
Printed: 03-Nov-97
at
01:10 PM
36
-------
Client: Pacific Environmental Services
Project Number: 43377
QA: Method Blank
TLI Samole ID:
Date Prepared:
Date Analyzed:
Matrix:
4TV77 MB
October 10-14. 1997
October 16.20.21 &22, 1997
N/A
Analyte
Aa
As
Ba
Be
Cd
Co
Cr
Cu
Mn
Ni
P
Pb
Sb
Se
' Tl
Zn
Method Blank
BeeosePKJ/l
AmoiMluaftf
-0.13
-2.09
020
0.01
-0.44
-0.19
-1.08
0.22
-0.19
-1.00
-0.70
-2.82
-1.10
-1.14
-0.10
7.27
^v VtS^tedfcft^^ '/*^">>x '
^ iMtiktitf ^v ';.*"
1
5
2
1
1
1
2
2
2
3
30
2
4
3
2
12
—
—
—
—
—
—
—
—
—
—
—
—
—
—
—
,-'- jftttaar ,
^'>T?1 **
Pass
Pass
Pass
Pass
Pass
Pass
Pass
Pass
Pass
Pass
Pass
Fail
Pass
Pass
Pass
Pass
—
—
—
—
—
—
—
—
—
—
—
—
—
—
—
Triangle Laboratories, Inc.
801 Capitola Drive * Durham, NC 2771
Tele: (919) 544-5729 * Fax: (919) 544-5491
Printed: 03-Nov-97
at
01:10PM
37
-------
Client: Pacific Environmental Services
Proiect Number: 43377
QA: Lab Control Spikes
TLI Sample ID:
Date Prepared: '
Date Analyzed:
Matrix:
43377 LCS
October 10-14. 1997
October 16.20.21 & 22. 1997
N/A
Anafrts
Aq
As
Ba
Be
Cd
Co
Cr
Cu
Mn
Ni
P
Pb
Sb
Se
Tl
Zn
Lab Control Soike
Ftecowered
A*rwun|fii($U
45.11
45.25
49.05
47.58
48.64
49.24
48.24
49.07
48.63
47.19
981.55
46.89
48.5t
47.66
45.00
199.45
Spike
Amount (MOflJ
50
50
50
50
50
50
50
50
50
50
1000
50
50
50
50
200
f
'f-;;%- ,
Fteoiaajjrv
90%
90°/c
98°/<
95°/c
97°/c
98%
96°/<
98°/t
97°/<
94%
98°/<
94°/c
97°/c
95°/c
90°/c
100°/c
Lab Control Soike Ducrficate
< ftecovemd
Amount ftKjf&
Sp8^^1
Afiwunltub'd
{, -% *!
FfeCOMKV
Fff*D
—
—
—
—
—
—
—
—
—
—
—
—
—
—
.„
—
—
—
—
—
—
—
...
—
—
—
—
—
...
—
—
Triangle Laboratories, Inc.
801 Capitola Drive * Durham, NC 27713
Tele: (919) 544-5729 * Fax: (919) 544-5491
Printed: 03-Nov-97
at
01:10 PM
33
-------
Client:
Proiect Nuitiher;
Pacific Environmental Services
- 43377
Sample Report
Page 1 of 4
Date Received:
Date Prepared:
Date Analyzed:
DATA FILE:
Matrix"
September 24. 1997
October 10-20. 1997
October 21-22. 1997
AB827 & AB828
Air
ANALYTE Ha
ua/LRDL: 0.2
AnaKttis Method:
29
Instrument PEZeeman 5100
SattaCenr fin/M S
CVAA ANALYTE SUMMARY REPORT
CSentQsHicteiD
O-M29-1-FHACE,FHAR,FILJER FH
O-M29-1-FHACE,FHAR,FILTER FH D
O-M29-1-HNO3BH
O-M29-1-HNO3BHD
O-M29-1-BHARHNO3
O-M29-1-BHARHNO3D
O-M29-1-KMnO4
O-M29-1-KMnO4D
O-M29-1-HQ
O-M29-1-HCID
O-M29-2-FHACE,FHAR,FILTER FH
O-M29-2-FHACE,FHAR,FILTER FH D
0-M29-2-HN03BH
O-M29-2-HNO3 BH D
O-M29-2-BHAR HNO3
O-M29-2-BHAR HNO3 D
O-M29-2-KMnO4
O-M29-2-KMnO4 D
O-M29-2-HCI
O-M29-2-HCI D
0-M29-3-FHACE,FHAR,FILJER FH
O-M29-3-FHACE,FHAR,FILTER FH D
0-M29-3-HNO3 BH
O-M29-3-HNO3 BH D
O-M29-3-BHAR HNO3
O-M29-3-BHAR HNO3 D
O-M29-3-KMnO4
O-M29-3-KMnO4 D
0-M29-3-HCI
O-M29-3-HCI D
mSAMffe' "^ -*
84-50-1 ABC
84-50-1 ABC D
84-50-10
84-50-1 DD
84-50-1 E
84-50-1ED
84-50-1 F
84-50-1 FD
84-50-1 G
84-50-1GD
84-50-2ABC
84-50-2ABC D
84-50-2DE
84-50-2DE D
184-50-2F
184-50-2F D
184-50-2G
184-50-2GD
184-50-2H
184-50-2H D
184-50-3ABC
184-50-3ABC D
184-50-3DE
184-50-3DE D
184-50-3F
184-50-3FD
184-50-3G
184-50-3GJD
184-50-3H
184-50-3HD
wafc-i
CONS
0.034
0.005
0.034
0.036
-0.005
-0.005
0.307
0.328
0.016
0.010
0.008
-0.008
0.034
0.023
•0.018
•0.016
0299
0.302
-0.021
-0.018
0.000
0.003
0.549
0.554
-0.003
-0.018
0.442
0.463
0.070
0.060
x«r
w
N/A
N/A
954
954
37
37
345
345
50
50
N/A
N/A
1645
1645
35
35
405
405
95
95
N/A
N/A
1130
1130
57
57
330
330
95
95
,«»
py
100
100
N/A
N/A
N/A
N/A
N/A
N/A
N/A
N/A
100
100
N/A
N/A
N/A
N/A
N/A
N/A
N/A
N/A
100
100
N/A
N/A
N/A
N/A
N/A
N/A
N/A
N/A
, fcU
ttksx*
5
5
5
5
5
5
5
5
5
5
5
5
5
5'
5
5
5
5
5
5
5
5
5
5
5
5
5
5
5
5
fflfiit
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
i->$>WMa
>fiB&o
< 0.400
< 0.400
< 3.82
< 3.82
< 0.148
< 0.148
2.12
225
< 0200
< 0200
< 0.400
< 0.400
< 6.58
< 6.58
< 0.140
< 0.140
2.42
2.45
< 0.380
< 0.380
< 0.400
< 0.400
12.4
12.5
< 0228
< 0228
2.92
3.06
< 0.380
< 0.380
< 0.400
< 3.82
< 0.148
2.19
< 0200
< 0.400
< 6.58
< 0.140
2.43
< 0.380
< 0.400
12.5
< 0.228
2.99
< 0.380
; >.*>•.
"WCt...
—
-
-
-
-
-
-
-
-
-
-
-
-
-
-
^ .••. vX
•KBEC;
-
-
-
-
-
-
-
-
-
-
-
—
-
-
"
39
-------
Client:
Project Number:
Pacific Environmental Services
Sample Report
Page 2 of 4
Date Received:
Date Prepared:
Date Analyzed:
DATA FILE:
Matrix*
Sentember 24. 1997
October 10-20. 1997
October 21-22. 1997
AB827 & AB828
Air
ANALVTE: Ho
0.2
Analysis Method:
29
Instrument PEZeaman 5100
Snike Cone. lua/L)
CVAA ANALYTE SUMMARY REPORT
CfentSaffloteS* " ' " •- *
0-M29-4-FHACE,FHAR,FILTER FH
O-M29-4-FHACE,FHAR,FILTER FH D
0-M29-4-HNO3 BH
O-M29-4-HNO3 BH D
O-M29-t-BHAR HNO3
O-M29^-BHAR HNO3 D
O-M29-4-KMnO4
O-M29-t-KMnO4 D
O-M29-4-HCI
O-M29-4-HCI D
O-M29-FB-FHACE,FHAR,FILTER FH
O-M29-FB-FHACE,FHAR,FILTER FH D
O-M29-FB-FHAR.HNO3 BH
O-M29-FB-FHAR.HNO3 BH D
O-M29-FB-BHAR HNO3
O-M29-FB-BHAR HNO3 D
0-M29-FB-KMnO4
O-M29-FB-KMnO4 D
0-M29-RB-FHACE,FHAR,FILTCR FH
O-M29-RB-FHACE.FHAR.FILTER FH D
O-M29-RB-FHAR.HNO3 BH
O-M29-RB-FHAR.HNO3 BH D
O-M29-RB-FHAR HNO3
O-M29-RB-FHAR HNO3 D
O-M29-RB-KMnO4
O-M29-RB-KMnO4 D
0-M29-RB-HCI
O-M29-RB-HCI D
iusAMpb* 5V
84-5CMABC
84-5CWABCD
84-504DE
84-50-4DED
84-50-4F
84-50-4FD
184-50-4G
184-50-4GD
184-50-4H
184-5CWHD
184-50-5ABC
184-50-5ABC D
184-50-5BD
184-50-5BDD
184-50-5E
184-50-5ED
184-50-5F
184-50-5F D
184-50-6ABC
184-50-6ABC D
184-50-6BD
184-50-6BD D
184-50-6B
1 84-50-68 D
184-50-6E
184-50-6ED
184-50-6FE
184-50-6FE D
#&-:>:
CC*fcr
-0.003
-0.016
0.026
0.029
0.018
0.000
0.299
0597
0.010
0.005
•0.003
-0.010
-0.016
-0.005
-0.013
-0.013
-0.018
•0.016
-0.016
-0.003
0.066
0.083
0.033
0.011
0.019
0.028
0.025
0.017
"-v'tt!
-w
N/A
N/A
1105
1105
56
56
350
350
61
61
N/A
N/A
150
150
56
56
155
155
N/A
N/A
300
300
100
100
290
290
94
94
,'W!
'FV
100
100
N/A
N/A
N/A
N/A
N/A
N/A
N/A
N/A
100
100
N/A
N/A
N/A
N/A
N/A
N/A
100
100
N/A
N/A
N/A
N/A
N/A
N/A
N/A
N/A
, ** -
A&NOt
5
5
5
5
5
5
5
5
5
5
5
5
5
5
5
5
5
5
5
5
5
5
5
5
5
5
5
5
^c&;
FACTOR
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
< 0.400
< 0.400
< 4.42
< 4.42
< 0224
< 0224
2.09
2.08
< 0244
< 0244
< 0.400
< 0.400
< 0.60
< 0.60
< 0224
< 0224
< 0.62
< 0.62
< 0.400
< 0.400
< 120
< 120
< 0.400
< 0.400
< 1.16
< 1.16
< 0.376
< 0.376
Qyt MT' 'i
S!**«HWIT:
< 0.400
< 4.42
< 0.224
2.09
< 0244
< 0.400
< 0.60
< 0.224
< 0.62
< 0.400
< 120
< 0.400
< 1.16
< 0.376
s\ \A
.f8P&..
_
-
-
-
-
-
-
-
-
-
-
-
-
-
•. '
ssrasbr
_
-
-
-
—
-
-
—
-
-
-
-
-
—
40
-------
Client:
Project Number;
Pacific Environmental Services
- 43377
Sample Report
Page 3 of 4
Date Received:
Date Prepared:
Date Analyzed:
DATA FILE:
Matrix:
Sentember 24. 1997
October 10-20, 1997
October 21-2Z 1997
AB827 A AB828
Air
ANALYTE: Ha
ua/LROL 0.2
Analysis Method:
instrument P E Zeenu
Suite Cone, fup/U
29
in 5100
5
CVAA ANALYTE SUMMARY REPORT
CtentSwraateSS: \%.
I-M29-1-FHACE,FHAR,FILTER FH
I-M29-1-FHACE,FHAR,FILTER FH D
I-M29-1-FHAR.HNO3 BH
I-M29-1-FHAR.HNO3 BH D
I-M29-1-FHARHNO3
I-M29-1-FHARHNO3D
l-M29-1-KMnO4
l-M29-1-KMnO4D
O-M29-1-HNO3BHMS
O-M29-1-HNO3BHMSD
0-M29-3-HNO3 BH MS
0-M29-3-HNO3 BH MSD
O-M29-4-HNO3 BH MS
O-M29-4-HNO3 BH MSD
O-M29-RB-FHAR.HNO3 BH MS
O-M29-RB-FHAR.HN03 BH MSD
I-M29-1-FHAR.HNO3 BH MS
I-M29-1-FHAR.HNO3 BH MSD
O-M29-1-HNO3BHMS
O-M29-1-HNO3BHMSD
O-M29-3-HNO3 BH MS
O-M29-3-HNO3 BH MSD
O-M29-4-HNO3 BH MS
O-M29-4-HNO3 BH MSD
O-M29-RB-FHAR.HNO3 BH MS
0-M29-RB-FHAR.HNO3 BH MSD
I-M29-1-FHAR.HNO3 BH MS
I-M29-1-FHAR.HN03 BH MSD
iiiaWL/J
184-50-7ABC
184-50-7ABC D
184-SO-7D
184-50-7D D
184-50-7E
184-50-7E D
184-50-7F
184-50-7F D
184-50-1 D MS
184-50-1 D MSD
184-50^3DE MS
184-50-3DE MSD
184-50-4DE MS
184-S04DE MSD
184-50-6BD MS
184-50-6BD MSD
184-50-7D MS
184-50-7D MSD
True Spike MS
True Spike MS
True Spike MS
True Spike MS
True Spike MS
True Spike MS
True Spike MS
True Spike MS
True Spike MS
True Spike MS
%«&?:
*&*&
0.075
0.063
0.166
0.144
0.022
0.011
0.075
0.072
8.522
8.504
8.403
7.976
7.750
7.575
4.937
5.227
4.424
5.125
5
5
5
5
5
5
5
5
5
5
•'$*.
-fV
N/A
N/A
435
435
85
85
275
275
954
954
1130
1130
1105
1105
300
300
435
435
954
954
1130
1130
1105
1105
300
300
435
435
\1fA
- *¥'
100
100
N/A
N/A
N/A
N/A
N/A
N/A
N/A
N/A
N/A
N/A
N/A
N/A
N/A
N/A
N/A
N/A
N/A
N/A
N/A
N/A
N/A
N/A
N/A
N/A
N/A
N/A
^ *ti -,
A&WOt
5
5
5
5
5
5
5
5
5
5
5
5
5
5
5
5
5
5
5
5
5
5
5
5
5
5
5
5
i'JPt.^
8*e$Qfl
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
T
-------
Client:
Project Number;
Pacific Environmental Services
' A33T7
Sample Report
Page 4 of 4
Date Received:
Date Prepared:
Date Analyzed:
DATA FILE:
Matrix:
September 24. 1997
October 10-20. 1997
October 21-22. 1997
AB827 & AB828
Air
ANALYTE Hq
uoA-RDL 0.2
Anatais Method
29
Instrument P E Teaman 5100
Sate Cpnc. (ua/L)
5
CVAA ANALYTE SUMMARY REPORT
CStentSoneteS^ ' '-' '''>'-" V
I-M29-1-FHAR.HNO3 BH MS
I-M29-1-FHAR.HN03 BH MSD
Method Blank
Method Blank D
.CS
_CSD
Method Blank
Method Blank 0
.CS
-CSD
* f &%$$$&&"'*''?*£
Tine Spike MS
Ttue Spike MS
43377 MB1
43377 MB1D
43377 LCS1
43377 LCS1D
43377 MB2
43377 MB2D
43377 LCS2
43377 LCS2D
^^
5
. 5
-0.008
-0.016
5278
5.018
0.003
-0.003
4.981
4.733
'3$
435
435
_
-
-
-
'$}:'
N/A
N/A
_
-
—
-
jAifQWt
5
5
^
-
-
-
1
1
^_
-
-
-
v&T«W«ff
*^iassuLJ
43.5
43.5
-
-
-
-
<*#w&*Hl
** ^ jMcsytiv^
-
mf
-
—
-
M
-
-
-
-
-
-
-
106%
100%
-
100%
95%
Triangle Laboratories, Inc.
301 Capitola Drive * Durham, North Carolina 27713
Tele: (919) 544-5729 * Fax: (919) 544-5491
Printed:
OS-Nov-97 at 0427PM
-------
O PACIFIC ENVIRONMENTAL SERVICES. INC.
Central Park West
5001 South Miami Boulevard, P.O. Box 12077
Research Triangle Park, North Carolina 27709-2077
(919) 941-0333 FAX: (919) 941-0234
Chain of Custody Record
•
>^l
CO
Project Numb
S4 13-004
Project Name PL MOT "A"
US EPA EMC Asphalt Cement,
Samplers: . '
Abemathy, Dickerson, Gay
Date
8/19/97
8/19/97
8/19/97
8/19/97
8/19/97
8/19/97
8/19/97
8/20/97
8/20/97
8/20/97
8/20/97
8/20/97
8/20/97
8/20/97
8/20/97
8/20/97
8/20/97
8/20/97
Time
1104
1104
, 1104
1104
1104
1104
1104
0822
0822
0822
0822
0822
0822
0822
1405
I 1405
1405
1405
Field Sample ID
i
O-M29-1-FHACE
Q-M29-1-FHAR
O-M29-1 -Filter
O-M29-1-HNO3
O-M29-1-BHAR
O-M29-1-KMnO4
O-M29-1-HCI
O-M29-2-FHACE
O-M29-2-FHAR
O-M29-2-Filter
O-M29-2-HNO3
O-M29-2-HNO3
O-M29-2-BHAR
O-M29-2-KMnO4
O-M29-2-HCI
O-M29-3-FHACE
O-M29-3-FHAR
O-M29-3-Filter
Relinquished by: (Signature)
I
Relinquished by: (Signature)
{
)e1im)tfched bvi (Signature)
Date/Time
Datefi"ime
Date/Time
tyt
Sample Description
FH Acetone Rinse - Beaker No. M-2
FH0.1 NHNO3 Rinse
Filter M97-003 - Beaker No, M-1
5% HNO3 / 10% H2O2 Absorbing Solution
BH0.1 NHNO3 Rinse
10% H2SO4 / 4% KMnO4 Absorbing Sol.
8N HCI Rinse
FH Acetone Rinse - Beaker No. M-5
FH 0.1 N HNO3 Rinse
Filter M97-002 - Beaker No. M-4
5% HN.O3 / 10% H2O2 Absorbing Solution
5% HNO3 / 10% H2O2 Absorbing Solution
BH0.1 NHNO3 Rinse
10% H2SO4 / 4% KMnO4 Absorbing Sol.
8N HCI Rinse
FH Acetone Rinse - Beaker No. M-7
FH 0.1 N HNO3 Rinse
Filter M97-004 - Beaker No. M-6
Received by: (Signature)
^
Deceived by: (Signature)
Received for lab bv: (Signature) ,
y^ifl.jfywt^
Analysis Requested
MM
•
•
•
•
•
*
•
•
•
•
•
•
•
•
Hg
•
•
•
•
•
•
•
•
•
•
•
•
•
*
•
•
•
•
» »f
Relinquished by: (Signature)
Relinquished by: (Signature)
Dale/Time
Date/Time
REMARKS
i
Remarks
.
Bottle 1/2
Bottle 2/2
Received by: (Signature)
Received by: (Signature)
_j_ —>
|Page:J of >
-------
£7 PACIFIC ENVIRONMENTAL SERVICES. INC.
Central Park West
5001 South Miami Boulevard, P.O. Box 12077
Research Triangle Park, North Carolina 27709-2077
(919)941-0333 FAX: (919) 941-0234
Chain of Custody Record
rf
4-
/
(
Project Numb
s41 3-004
Project Name pi_* «J
US EPA EMC Asphalt Cement,
T- ,. An
Samplers:
Abemathy, Dickerson, Gay
Date
8/20/97
8/20/97
8/20/97
8/20/97
8/20/97
8/21/97
8/21/97
8/21/97
• 8/21/97
8/22/97
8/21/97
8/21/97
8/21/97
8/20/97
8/20/97
8/20/97
8/20/97
8/20/97
Time
1405
1405
1405
1405
1405
0740
0740
0740
0740
0741
0740
0740
0740
•*
Field Sample ID
Q-M29-3-HNO3
O-M29-3-HNO3
O-M29-3-BHAR
O-M29-3-KMnO4
O-M29-3-HCI
O-M29-4-FHACE
O-M29-4-FHAR
O-M29-4-Filter
0-M29-4-HNO3
0-M29-4-HNO4
O-M29-4-BHAR
O-M29-4-KMnO4
O-M29-4-HCI
0-M29-FB-FHACE
O-M29-FB-FHAR
O-M29-FB-Filter
O-M29-FB-HNO3
O-M29-FB-BHAR
Relinquished by: (Signature)
I
Relinquished by: (Signature)
\
' \
Fftlinmtithftd hi
riBiinmiisraw r,
\)U.
y(Sigyature)
IT .
Date/Time
Date/Time
OateH'trne
zlxfa
' mo
Sample Description
5% HNO3 / 10% H2O2 Absorbing Solution
5% HN03 / 10% H2O2 Absorbing Solution
BH0.1 NHNO3 Rinse
10% H2S04 / 4% KMnO4 Absorbing Sol.
8N HCI Rinse
FH Acetone Rinse - Beaker No. M-9
FH 0.1 N HNO3 Rinse
Filter M97-005 - Beaker No. M-8
5% HN03 / 10% H202 Absorbing Solution
5% HNO3 / 10% H2O2 Absorbing Solution
BH0.1 NHN03 Rinse
10% H2S04 / 4% KMnO4 Absorbing Sol.
8N HCI Rinse
FH Acetone Rinse - Beaker No. M-15
FH0.1 NHN03 Rinse
Filter M97-006 - Beaker No. M-14
5% HN03 / 10% H202 Absorbing
BH 0.1 N HNO3 Rinse
Received by: (Signature)
i
deceived by: (Signature)
Received for lab by: (Signature) .
Solution
Analysis Requested
MM
Hg
• »,
Relinquished by: (Signature)
Relinquished by: (Signature)
Date/Time
DatefTime
REMARKS
Remarks
Bottle 1/2
Bottle 2/2
Bottle 1/2
Bottle 2/2
Received by: (Signature) '
Received by: (Signature)
^^^^^^^^^ • **
|Page: «- of S
-------
PACIFIC ENVIRONMENTAL SERVICES. INC.
Central Park West
5001 South Miami Boulevard, P.O. Box 12077
Researqh Triangle Park, North Carolina 27709-2077
(919) 941-0333 FAX: (919) 941-0234
Chain of Custody Record
•
cr<
Project Numb
s4 13-004
Project Name PLA-MT " /*, "
US EPA EMC Asphalt Cement.
Samplers:
Abernalhy, Dickerson, Gay
Dale
8/20/97
8/20/97
8/21/97
8/21/97
8/21/97
8/21/97
8/21/97
. 8/21/97
8/19/97
8/19/97
8/19/97
8/19/97
8/19/97
8/19/97
,
Time
I
*
•'
' 1
Field Sample ID
O-M29-FB-KMnO4
O-M29-FB-HCI
O-M29-RB-FHACE
O-M29-RB-FHAR
O-M29-RB-Filter
0-M29-RB-HN03
O-M29-RB-KMnO4
O-M29-RB-HCI
-M29-1-FHACE
-M29-1-FHAR
-M29-1 -Filter
-M29-1-HNO3
-M29-1-BHAR
-M29-1-KMnO4
Relinquished by: (Signature)
/~\ \
lR*linqblshed bv: (Signature)
rrVy r
\ L^f Af
Date/Time
DateHVne
Sample Description
10% H2SO4 / 4% KMnO4 Absorbing Sol.
8N HCI Rinse
FH Acetone Rinse - Beaker No. M-18
FH0.1 NHNO3 Rinse
Filter No. 97-001 - Beaker No. M-16
5% HNO3 / 10% H2O2 Absorbing Solution^
10% H2SO4 / 4% KMnO4 Absorbing Sol.
8N HCI Solution
FH Acetone Rinse - Beaker No. M-1 1
FH0.1 NHNO3 Rinse
Filter M97-0010 - Beaker No. M-10
5% HNO3 / 10% H202 Absorbing Solution
BH0.1 NHNO3 Rinse
10% H2SO4 /4% KMn04 Absorbing Sol.
'
Received by: (Signature)
Received by: (Signature)
Analysis Requested
MM
Hg
Relinquished by: (Signature)
Relinquished by: (Signature)
Date/Time
DatefTlme
>•
Remarks
Received by: (Signature)
Recetod by: (Signature)
-------
U U t v
=TRIANGLE LABORATORIES, INC.
Cf " •'f <• /
LOG IN RECORD/CHAIN OF CUSTODY=
Custody Seal : Absent Sample Seals : Absent
Chain of Custody : Present Container...: Intact
Sample Tags : Absent
Sample Tag Numbers: Not Listed on Chain of Custody
SMO Forms : N/A
TLI Project Number 43377 , | Book ||
Client: PES03 - Pacific Environmental Services' | ||
yJ-X / • 44 \t./f JJ,
Date Received | 09/24/97 | By^£^t^jf 4//tt^fa>Pt$^&.
|| i j, , M
Ice Chest NO COOLANT Temp 20 . 0 C Carrier and Number | HAND DELIVERED f \ 50 U
JTIiI Number Client Sample ID Matrix
jimR/H-CPM Client COC ID * Location
-'"
||184-SO-1A 0-M29-1-FHACE FH ACETONE RINSE
|| O-M29-1-FHACE METALS LAB
"
||184-50-1B O-M29-1-FHAR FH .IN HNO3
|| O-M29-1-FHAR METALS LAB
,
||184-50-1C O-M29-1-F,ILTER FILTER
|| 0-M29-l-FtLTER METALS LAB
||184-50-1D O-M29-1-HN03 HN03/H2O2
|| O-M29-1-HNO3 METALS LAB
,_., ,
D184-50-1E 0-M29-1-BHAR BH HNO3
I) O-M29-1-BHAR METALS LAB
IJ184-SO-1F O-M29-1-KMN04 H2S04/KMN04
|| 0-M29-1-KMN04 METALS LAB
1)184-50-10 O-M29-1-HCL BN HCL
|| 0-M29-1-HCL METALS LAB
||184-50-2A O-M29-2-FHACE FH ACETONE RINSE
1) O-M29-2-FHACE METALS LAB
||184-50-2B O-M29-2-FHAR FH .IN HNO3
U O-M29-2-FHAR METALS LAB
•
||184-50-2C O-M29-2-FILTER FILTER
O-M29-2-FILTER METALS LAB
184-50-2D O-M29-2-HNO3 HN03/H202
0-M29-2-HN03 METALS LAB
184-50-2E 0-M29-2-HN03 HN03/H202
O-M29-2-HN03 METALS LAB
JJ184-50-2F O-M29-2-BHAR BH HNO3
I 0-M29-2-BHAR METALS LAB
To LAB
Date/Init
'-
£«4-50-2G 0-M29-2-KMN04 H2S04/KMNO4J
J-) 0-M29-2-KMN04 METALS LAB |
To STORAGE
Date/Init
'
To LAB
Date/Init
To STORAGE
Date/Init
.
1
TO LAB
Date/Init
....
To STORAGE
Date/Init
1
•*
| 1
1
.
To LAB
Date/Init
1 . 1
| 1
1 1
„, . .
1
1 1
To STORAGE
Date/Init
i.
,
.
1
' 1
— 1
| j
DISPOSED
Date/Init
1
•
II Receiving Remarks: NO COOLANT WAS WITH SAMPLES. COC LISTED SAMPLE O-M29-FB-HCL BUT SAMPLE WAS NOT RECEIVED.
II
II
II Archive Remarks :
•Form Revised 05/27/1997 -- Page 1 OF 4«
-------
TRIANGLE LABORATORIES, INC. -- LOG IN RECORD/CHAIN OF CUSTODY=
|| Custody Seal : Absent Sample Seals: Absent
U Chain of Custody : Present Container...: Intact
H Sample Tags : Absent
|| Sample Tag Numbers: Not Listed on Chain of Custody
I) SMO Forms : N/A
TLI Project Number 43377 , | Book
Client: PES03 - Pacific Environmental Services j
*S J, 184
Date Received j 09/24/97 j ByX^^J^ J^£ fifol&^
II I • j |
D Ice Chest NO COOLANT Temp 20.0 C Carrier and Number | HAND DELIVERED ( j SO
flTLI Number Client Sample ID Matrix) To LAB
HmR/H:CPM. Client COC ID . . * Location j Date/Init
II 1
J1S4-50-2H 0-M29-2-HCL 8N HCL|
Q 0-M29-2-HCL METALS LAB |
II 1
H184-50-3A 0-M29-3-FHACE FH ACETONE RINSE)
|| O-M29-3-FHACE METALS LAB j
nj
||184-SO-3B O-M29-3-FHAR FH .IN HNO3 1
11 O-M29-3-FHAR METALS LAB j
II 1
U184-50-3C O-M29-3-FILTER ' ' FILTER)
1) O-M29-3-FILTER METALS LAB |
II 1
||184-50-3D 0-M29-3-HN03 HN03/H202 1
|| O-M29-3-HNO3 METALS LAB j
II 1
||184-50-3E 0-M29-3-HN03 HNO3/H2O2)
U 0-M29-3-HN03 METALS LAB j
I) .. . 1
||184-50-3P 0-M29-3-BHAR BH HN03 1
\ O-M29-3-BHAR METALS LAB j
It , ... ,„_.,,.. 1
1)184-50-30 O-M29-3-KMN04 H2SO4/KMNO4 1
IJ O-M29-3-KMN04 METALS LAB j
g . _ ,._ .. . j
||184-50-3H 0-M29-3-HCL 8N HCL|
1) 0-M29-3-HCL METALS LAB |
IJ „.. |
J184-50-4A 0-M29-4-FHACE FH ACETONE RINSE|
| O-M29-4-FHACB METALS LAB j
g 1
||184-SO-4B 0-M29-4-FHAR FH .IN HN03 1
IJ 0-M29-4-FHAR METALS LAB j
II I
||184-50-4C 0-M29-4-FILTER FILTER]
|| 0-M29-4-FILTER METALS LAB j
II
II i
||184-SO-4D O-M29-4-HNO3 HNO3/H202)
U 0-M29-4-HN03 • METALS LAB j
|| - |
JJ184-50-4E 0-M29-4-HN03 HNO3/H2O2|
>fir ' 0-M29-4-HN04 * METALS LAB j
To STORAGE
| Date/Init
| To LAB
Date/Init
To STORAGE
Date/Init
| To LAB
Date/Init
To STORAGE
Date/Init
*
*
•
| To LAB
Date/Init
1
1
i
I
To STORAGE
Date/Init
i.
| 1
-••
| DISPOSED
Date/Init .
• .
i * •
D
|| Receiving Remarks: NO COOLANT WAS WITH SAMPLES. COC LISTED SAMPLE O-M29-FB-HCL BUT SAMPLE WAS NOT RECEIVED.
II
II
|| Archive Remarks :
=Form Revised 05/27/1997 -- Page 2 OF 4
-------
=TRIANGLE LABORATORIES, INC. -- LOG IN RECORD/CHAIN OF CUSTODY=
|| Custody Seal : Absent Sample Seals: Absent
|| Chain of Custody : Present Container....- Intact
|| Sample Tags : Absent
|| Sample Tag Numbers : Not Listed on Chain of Custody
II SMO Forms : N/A
TLI Project Number 43377 . | Book
Client: PES03 - Pacific Environmental Services |
1 "4
f J t . Jif ,^|
Date Received j 09/24/97 j BJ^^^$^<#£JV*^
|| Ice Chest NO COOLANT Temp 20.0 C Carrier and Number | HAND DELIVERED ' \ 50
IJTI.I Number.. .. Client Sample ID Matrix
jjmR/H-CPM Client COC ID * Location
||184-SO-4F O-M29-4-BHAR BH HN03
|| O-M29-4-BHAR METALS LAB
»-
||184-SO-4O 0-M29-4-KMN04 H2SO4/KMN04
D O-M29-4-KMNO4 METALS LAB
H1
)|184-50-4H 0-M29-4.-HCL 8N HCL
|j 0-M29-4>-HCL METALS LAB
||1B4-50-5A ' O-M29-FB-FHACE FH ACETONE RINSE
IJ O-M29-FB-FHACE METALS LAB
||1B4-SO-SB O-M29-FB-FHAR FH .IN HNO3
|| O-M29-FB-FHAR METALS LAB
||
||184-SO-SC O-M29-FB-FILTER FILTER
|| O-M29-FB-FILTER METALS LAB
H184-50-5D 0-M29-FB-HN03 HNO3/H2O2
j| 0-M29-FB-HNO3 METALS LAB
||184-50-5E 0-M29-FB-BHAR BH HNO3
IJ O-M29-FB-BHAR METALS LAB
||184-SO-5F 0-M29-FB-KMN04 H2SO4/KMNO4
IJ O-M29-FB-KMNO4 METALS LAB
||184-50-€A 0-M29-RB-FHACE FH ACETONE RINSE
IJ O-M29-RB-FHACE METALS LAB
||184-50-6B 0-M29-RB-FHAR FH .1 HN03
H 0-M29-RB-FHAR METALS LAB
R1B4-50-6C 0-M29-RB-FILTER FILTER
|| O-M29-RB-FILTER METALS LAB
II
||184-50-6D 0-M29-RB-HN03 HN03/H2O2
|| 0-M29-RB-HN03 METALS UAB
To LAB
Date/Init
'"
II
||184-50-6E 0-M29-RB-KMN04 H2S04/KMNO4|
Jb» ' 0-M29-RB-KMN04 METALS LAB j
To STORAGE
Date/Init
To LAB
Date/Init
To STORAGE
Date/Init
To LAB
Date/Init
To STORAGE
Date/Init
To LAB
Date/Init
1
\
I
To STORAGE
Date/Init
''
...
- ^ 1
DISPOSED
Date/Init
1
I
II
1
T| Receiving Remarks: NO COOLANT WAS WITH SAMPLES. COC LISTED SAMPLE O-M29-FB-HCL BUT SAMPLE WAS NOT RECEIVED. ,
Archive Remarks:
-------
=TRIANGLE LABORATORIES, INC. -- LOG IN RECORD/CHAIN OF CUSTODY=
I) Custody Seal : Absent Sample Seals: Absent
|| Chain of Custody : Present Container. . . : Intact
|| Sample Tags : Absent
U Sample Tag Numbers: Not Listed on Chain of Custody
I) SMO Forms : N/A
TLI Project Number 43377 . Book 1
Client: PES03 - Pacific Environmental Services'
i 184
Date Received j 09/24/97 j By l<. Page
i i li
II i (j
|| Ice Chest NO COOLANT* Temp 20 . 0 C Carrier and Number | HAND DELIVERED ( 50
||TLI Number Client Sample ID Matrix
j|mR/H:CPM. Client COC ID * Location .
U
||184-50-6F O-M29-RB-HCL BN HCL
IJ O-M29-RB-HCL METALS LAB
ft
||184-50-7A , I-M29-1-FHACE FH ACETONE RINSE
jj I-M29-1-FHACE METALS LAB
||184-50-7B I-M29-1-,FHAR FH .IN HNO3
II I-M29-1-FHAR METALS LAB
||184-50-7C I-M29-1-FILTER FILTER
II I-M29-1-FILTER METALS LAB
H
||184-50-7D I-M29-1-HNO3 HN03/H2O2
|| I-M29-1-HNO3 METALS LAB
H
||184-SO-7E I-M29-1-BHAR BH HNO3
i I-M29-1-BHAR METALS LAB
||184-SO-7F , I-M29-1-KMNO4 H2SO4/KMNO4
D I-M29-1-KMNO4 METALS LAB
1
1
To LAB
Date/Init
-
,
„.._
To STORAGE
Date/Init
To LAB
Date/Init
To STORAGE
Date/Init
| To LAB
Date/Init
To STORAGE
Date/Init
V
I TO 'LAB
Date/Init
To STORAGE
Date/Init
'•
1
—-\
I DISPOSED
Date/Init
1
i
1 a
|| Receiving Remarks: NO COOLANT WAS WITH SAMPLES. COC LISTED SAMPLE 0-M29-FB-HCL BUT SAMPLE WAS NOT RECEIVED. 1
II
II
|| Archive Remarks:
=Form Revised 05/27/1997 -- Page 4 OF 4=
-------
3roJecM/
Client:
4 AW
j' Iv _-~
Triangle Laboratories of RTF
(919) 544-5729
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