-------
2 . ID: 184-84-4D
plicate 1
ak Area (A-s): 0.045
ank Corrected Pk Height (A): 0.002
ncentration (ug/L ): 0.026
Seq. No.: 00066 A/S Pos.: - Date: 10/20/97
Tiie: 14:39
Peak Height (A): 0.002
2 ID: 184-84-40 D • Seq. Ho.: 00067 A/S Pos.: -- Date: 10/20/97
plicate 1 Ti»e: 14:40
ak Area (A-s): 0.030 Peak Height (A): 0.001
ank Corrected Pk Height (A): 0.001
ncentration (ug/L ): 0.016
I ID: 184-84-4D MS Seq/ No.: 00068 A/S Pos.: - Date: 10/20/97
jlicate 1 Tine: 14:41
ik Area (A-s): 4.079 Peak Height (A): 0.168
ank Corrected Pk Height (A): 0.168
icentration (ug/L ): 2.599
I ID: 184-84-4D USD Seq. No.: 00069 A/S Pos.: -- Date: 10/20/97
Jlicate 1 Time: 14:42
Jk Area (A-s): 4.112 Peak Height (A): 0.170
ink Corrected Pk Height (A): 0.170
icentration (ug/L ): 2.631
1 ID: 184-84-4E Seq. No.: 00070 A/S Pos.: - Date: 10/20/97
licate 1 Tine: 14:43
k Area (A-s): 0.096 Peak Height (A): 0.004
nk Corrected Pk Height (A): 0.004
centration (ug/L ): 0.061
ID: 184-84-4E D Seq. No.: 00071 A/S Pos.: - Date: 10/20/97
licate 1 Time: 14:44
k Area (A-s): 0.073 Peak Height (A): 0.003
nk Corrected Pk Height (A): 0.003
centration (ug/L ): 0.048
ID: 184-84-4F
licate 1
( Area (A-s): 0.010
ik Corrected Pk Height (A): 0.001
:entration (ug/L ): 0.011
Seq. No.: 00072 A/S Pos.: -- Date: 10/20/97
Tine: 14:45
Peak Height (A): 0.001
145
-------
Peak 'Area (A-s): 0.006 Peak Height (A): 0.001
Blank Corrected Pk Height (A): 0.001
Concentration (ug/L ): 0.012
-
Hg2 ID: 184-84-5CW ^...^Se^. Ho.: 00074 A/S Pos.: -• Date: 10/20/97
Replicate 1 Tiie: 14:47
Peak Area (A-s): 0.004 Peak Height (A): 0.000
Blank Corrected Pk Height (A): 0.000
Concentration (ug/L ): 0.005
,«.«,.^^...,.««...,^^.^^.
Hg2 ID: 184-84-5CA6 D Seq. No.: 00075 A/S Pos.: - Date: 10/20/97
Replicate 1 Tine: 14:49
Peak Area (A-s): 0.001 " Peak Height (A): 0.000
Blank Corrected Pk Height (A): 0.000
Concentration (ug/L ): 0.002
Hg2 ID: CCV5:6.0ug/L Seq. No.: 00076 A/S Pos.: -- Date: 10/20/97
Replicate 1 Time: 14:50
Peak Area (A-s): 8.459 Peak Height (A): 0.354
Blank Corrected Pk Height (A): 0.354
Concentration (ug/L ): 5.495
Hg2 ID: CCB5 Seq. No.: 00077 A/S Pos.: -- Date: 10/20/97
Replicate 1 Tine: 14:51
Peak Area (A-s): 0.029 Peak Height (A): 0.001
Blank Corrected Pk Height (A): 0.001
Concentration (ug/L ): 0.017
Hg2 ID: 184-84-5BD Seq. No.: 00078 A/S Pos.: -- Date: 10/20/97
Replicate 1 Time: 14:52
Peak Area (A-s): 0.014 Peak Height (A): O.OOi
Blank Corrected Pk Height (A): 0.001
Concentration (ug/L ): 0.012
Hg2 ID: 184-84-5BD D Seq. No.: 00079 A/S Pos.: - Date: 10/20/97
Replicate 1 Tiie: 14:53
Peak Area (A-s): 0.006 Peak Heighf{A): 0.00.
Blank Corrected Pk Height (A): 0.001
Concentration (ug/L ): 0.009
Hg2 ID: 184-84-5E Seq. No.: 00080 A/S Pos.: - Date: 10/20/97
Replicate 1
Tiie: 14:55
n..t. It*. £ _L A / A
146
-------
I ID: 184-84-5E D Seq. No.: 00081 A/S Pos.: - Date: 10/20/97
)licate 1 Tiae: 14:56
ik Area (A-s): -0.003 Peak Height (A): -0.000
ink Corrected Pk Height (A): -0.000
icentration (ug/L ): -0.002
! ID: 184-84-5F Seq. No.: 00082 A/S Pos.: -- Date: 10/20/97
>licate 1 Tine: 14:57
•.k Area (A-s): -0.001 Peak Height (A): -0.000
ink Corrected Pk Height (A): -0.000
centration (ug/L ): -0.003
ID: 184-84-5F D Seq. No.: 00083 A/S Pos.: - Date: 10/20/97
•licate 1 Tine: 14:58
k Area (A-s): 0.000 Peak Height (A): 0.001
nk Corrected Pk Height (A): 0.001
centration (ug/L ): 0.008
ID: 184-84-5GF Seq. No.: 00084 A/S Pos.: -- Date: 10/20/9*
licate 1 Tine: 14:59
k Area (A-s): 0.036 Peak Height (A): 0.002
nk Corrected Pk Height (A): 0.002
centration (ug/L ): 0.026
ID: 184-84-5GF D Seq. No.: 00085 A/S Pos.: -- Date: 10/20/9"
licate 1 Time: 15:00
k Area (A-s): 0.015 Peak Height (A): 0.001
nk Corrected Pk Height (ft): 0.001
centration (ug/L ): 0.008
ID: CCV6:6.0ug/L Seq. No.: 00086 A/S Pos.: -- Date: 10/20/9"
licate 1 Tine: 15:01
k Area (A-s): 6.713 Peak Height (A): 0.284
nk Corrected Pk Height (ft): 0.284
centration (ug/L ): 4.407
ID: CCV6:6.0ug/L Seq. No.: 00087 A/S Pos.: - Date: 10/20/97
licate 1 Tine: 15:06
k Area (A-s): 5.871 Peak Height (A): 0.254
nk Corrected Pk Height (A): 0.254
:entration (ug/L ): 3.932
147
-------
Replicate 1 Tiie: 15:17
Peak Area (A-s): 5.836 Peak Height (A): 0.263
Blank Corrected Pk Height (A): 0.263
Concentration (ug/L ): 4.073
Hg2 ID: CCB6 Seq. No.: 00089 A/S Pos.: - Date: 10/20/97
Replicate 1 Tiie: 15:19
Peak Area (A-s): -0.006 Peak Height (A): -0.000
Blank Corrected Pk Height (A): -0.000
Concentration (ug/L ): -0.002
148
-------
(eight File: A8827.IDH Analyst: O.STREETER-EOHARDS
>le Volune: 100 iL Noninal Weight: 1.0 g
>c. Saaple ID " Weight Dilution
0 ST 81K
1 8101:0.2119/1^
2 STD2:0.5ug/L
3 STD3--1.0ug/L \^
4 5TD4:2.0ug/L f
5 STD5:5.0ug/l I
6 5T06:lO.Oug/L 1
7 ICV:4.0ug/l IL__ 1 625-b KG
8 .IC8
9 CHECK LO
0 43411 M82
1 43411 M820
2 43411 LCS2.
3 43411 LCS2D
4 184-84-6CA8
5 184-84-6CAB D
6 184-34-60
7 184-84-60 D
8 184-34-60 MS ,-•;'. ••' ; ',
9 184-84-60 USD
0 CCV7:6.0ug/L 3-033-C*
1 CCB
2 134-S4-6G
3 184-34-6G D
4 1S4-34-5E
5 184-34-6E D
5 184-34-oF
7 184-84-6F D
3 1S4-34-7CDA8
9 184-84-7COAB D
) 184-34-7G
1 134-84-7G D
I CCVS:6.0ug/L
i CCB
< 1S-1-84-7EF
5 184-84-7EF D
5 184-84-7EF MS
1 1S4-84-7EF MSD
3 184-34-7H
» 184-84-7H D
) 184-34-71
I 184-84-71 D
I CCV9:6.0ug/L —
i 43377 MSI
t 43377 M81 D
i 43377 LCS1
. 43377 LCS10
184-50-1CAB
! 184-50-1CA8 0
184-50-10
184-50-10 D
184-50-10 MS
184-50-10 MSO
CCVl:6.0ug/L —
149
-------
Loc. Saiple ID Weight . Dilution
54
55
56
57
58
59
60
61
62
63
64
65
66
67
68
69
70
71
72
73
74
75
76
77
73
79
SO
81
32
83
84
85
86
87
88
89
90
91
92
93
94
95
96
97
93
99
100
101
102
103
104
105
106
107
108
109
CCS ' -
184-50-1E
184-50-1E 0
184-50-1F
184-50-1F 0
184-50-16
184-50-1G 0
184-50-2CA8
184-50-2CA8 0
184-50-20E
184-50-20E 0
CCV2=6.0ug/L —3-Ofo-b "Kf lo
CC8
184-50-2F
184-50-2F 0
184-50-26 '
184-50-26 D
184-50-2H
184-50-2H 0
184-50-30E
184-50-30E 0
184-50-30E MS
184-50-30E MSO
CCV3:6.0ug/L 3-6^3-U fr5E 1
CCS
184-50-3CAB
1S4-50-3CA8 0
184-50-3F
184-50-3F 0
184-50-36
134-50-3G 0
184-50-3H
184-50-3H D
184-50-4CA8
184-50-4CA8 0
CCV4:6.0ug/l 3-0^3-1(2. D5€
CCS
184-50-4DE
184-50-40E 0
184-50-4DE MS
184-50-40E HSO
184-50-4F
184-50-4F 0
184-50-46
134-50-46 D
184-50-4H
184-50-4H 0
CCV5=6.0ug/L - 3_x*o.?/
pro ^ ~" O (A jrty
w WL
184-50-5CA8
184-50-5CA8 0
184-50-580
184-50-5BD D
184-50-5E
184-50-5E D
184-50-5F
150
-------
Sanole ID Weight Dilution
0 184-50-5F D
1 184-50-6CAB
2 184-50-6CAB D
3 CCV6:6.0ug/L
4 CCS
151
-------
Eleneat: Hg2
Print Data: Main+Suppl.
Print: Calib. Curve
Resarks:
STANDARDS: 3-023-5
QC: 3-023-4.1,
INSTRUMENT: 5100
Wavelength: 253.7 Peak
Signal Type: AA
Read Time: 30.0
Sanple Replicates: 1
Standard Replicates: 1
Calibration Type: Linear
QC:
Matrix. Check Calculations:
% Difference for Dupls: No
* Recovery for Spike: No
Analyst: 0 3TREETER-EDHAROS
Peak -Storaae: Hone
Technique: MHS Version: 7.01
Slit: 0.7 Low
Signal Measurement: Peak Height (5)
Read Delay: 1.0 BOC Tine: 2
FLAME:
Flaae Type:
Oxidant Flow
CALIBRATION:
Solutions
Calib. Blank
Standard 1
Standard 2
Standard 3
Standard 4
Standard 5
Standard o
Calibration
Air
: 10.0 L/nin
1 ID
, i IU Olr\
ISTD i
ISTD 2
ISTD 3
ISTD 4
ISTD 5
ISTO 6
Units: ug/L
Flame Sensor
Fuel Flow: 2
Cone |
1
1
0.2001
0.5001
1.0001
2.0001
5.000',
10.000,'
Sample Units
: On
.0 l/nin
: ug/L
Lo:a:ions:
Locations:
ujnc:
152
-------
lent File: HG..MEL Eleient: Hg? Wavelength: 253.
i: 10/21/97. . Tiie: 10:09 Slit: 0.7 L
File: AB827.DAT ID/Wt File: AB827.IDW La»p Current: 0
mique: MHS Calib. Type: Linear Energy: 71
.rk 1: STANDARDS: 3-023-5
,rk 2: QC: 3-023-4;o
ID: ST 8LK
Seq. Ho.: 00003 A/S Pos.: -- Date: 10/21/97
icate 1 Tine: 10:10
Area (A-s): -0.004 Peak Height (A): -0.000
k Corrected Pk Height (A): -0.000
entration (ug/L ):"-0.003
-zero performed.
ID: STDl:0.2ug/L
Seq. No.: 00004 A/S Pos.": -- Date: 10/21/9'
icate 1 Tine: 10:11
Area (A-s): 0.170 Peak Height (A!: 0.007
k Corrected Pk Height (A): 0.007
sntration (ug/L ): 0.107
jard number 1 apolied. [0.200]
slation coefficient: 1.00000 Slope: 0.054o
ID: 5TD2--0.5uo/L
Sea. No.: OCOOS A/£ Pos.: -- Date: 10/21/9'
le abs. is greater than that of the largest standarc.
icate 1 Tine: 10:12
Area (A-s): 0.395 Peak Height (A): 0.013
< Corrected Pk Height (A): O.Ole
antration (ug/L ): 0.525
Jard number 2 applied. [0.500]
elation coefficient: 0.99914 Slope: 0.0561
ID: STD3=1.0uo/L
Seq. No.: 00006 A/S Pos.: -- Date: 10/21/97
le abs. is greater than that of the largest standard.
icate 1 Tine: 10:13
Area (A-s): 0.878 Peak Height (A): 0.039
< Corrected Pk Height (A): 0.039
miration (ug/L ): 1.073
fard number 3_applied. [1.000]
ilation coefficient: 0.99824 Slope: 0.0382
ID: STD4:2.0ug/L
Seq. No.: 00007 A/S Pos.: -- Date: 10/21/9'
e abs. is greater than that of the largest standard.
cate 1 Ti«e: 10:15
Area (A-s): 1.761 Peak Height (A): 0.774
153
-------
Eleaent File: HG..MEL Eleunt: Hg2
Date: 10/21/97 - Tiae: 10:09
Data File: AB827.DAT ID/HI File: AB827.IDW
Technique: MHS lalib. Type: Linear
Reaark 1: STANDARDS: 3-023-5
Reaark 2: QC= 3-023-4,
Havelength: 253.
Slit: 0.7 L
Laap Current: 0
Energy: 71
Hg2 ID: ST BLK
Seq. No.: 00003 A/S Pos.: -- Date: 10/21/97
Replicate 1 Tiie: 10:10
Peak Area (A-s): -0.004 Peak Height (A): -0.000
Blank Corrected Pk Height (A): -0.000
Concentration (ug/L ): -0.003
Auto-zero perforaed.
Hg2 ID: STDl=0.2ug/l
Seq. No.: 00004 A/S Pos.: •-• Date:.10/21/r
Replicate 1 Time: 10:11
Peak Area (A-s): 0.170 Peak Height (A): 0.007
Blank Corrected Pk Height (A): 0.007
Concentration (ug/L ): 0.107
Standard number 1 applied. [0.200]
Correlation coefficient: 1.00000 Slope: 0.034o
Hg2 ID: 5102=0.5ug/L
Seq. No.: 00005 A/£ Pos.: - Oats: 10.'21'9'
Sample abs. is greater than that of the largest standard.
Replicate 1 Tine: 10:12
Peak Area (A-s): 0.395 Peak Height (A): 0.013
Blank Corrected Pk Height (A): O.Olc
Concentration (ug/L ): 0.525
Standard number 2 applied. [0.500]
Correlation coefficient: 0.99914 Slope: 0.036,
Hg2 ID: 5TD3=1.0ug/L
Seq. No.: 00006 A/S Pos.: -- Date: 10/21/97
Sarople abs. is greater than that of the largest standar:.
Replicate 1 Tine: 10:15
Peak Area (A-s): 0.878 Peak Height (A): 0.03?
Blank Corrected Pk Height (A): 0.039
Concentration (ug/L ): 1.073
Standard number 3 applied. [1.000]
Correlation coefficient: 0.99824 Slope: 0.038?
Hg2 ID: STD4:2.0ug/L Seq. No.: 00007 A/S Pos.: -- Date: 10/21/9"
Sasple abs. is greater than that of the largest standard.
Replicate 1 Tine: 10:15
Peak Area (A-s): 1.761 Peak Height (A): 0.074
154
-------
k.Corrected Pk Height !A): 0.074
entration i.ug/L ): 1.9*3
oara number 4 applied. [2.000]
elation coefficient: 0.99947 Slope: 0.0373
10: STD5:5.0ug/L S.eq. No.: 00003 A/S Pos.: -- Date: 10/21/97
le abs. is greater than that of the largest standard.
icate 1 Time: 10:16
Area (A-s): 4.444 Peak Height (A): 0..190
< Corrected Pk Height (A): 0.190
entration (ug/L ): 5.088
iard number 5 applied. [5.000]
ilation coefficient: 0.99989 Slope: 0.0379
ID: STD6:10.0ug/l Seq. No.: 00009 A/S Pos.: -- Date:" 10/21/9'
.e abs. is greater than that of the Urges: standard.
.cats 1 Time: 10:P
Area (A-s): 5.952 Peak Height (£j: 0.333
; Corrected Pk Height (A): 0.33S
mtration (ug/L ): 10.231
lard number 6 applied. [10.000]
ilation coefficient: 0.99389 Sloce: 0.0356
155
-------
Blank .Corrected Pk Height (A): 0.07*
Concentration i.ug/'l ): 1.943
Stanoan number 4 applied. [2.000]
Correlation coefficient: 0.99947 Slope: 0.0373
Hg2 10: 3105=5.Qug/l 5.eq. No.: 00003 A/S Pos.: - Date: 10/21/97
Sample abs. is greater than that of the largest standard.
Replicate 1 Tine: 10:16
Peak Area (A-s): 4.444 Peak Height (A): 0..190
Blank Corrected Pk Height (A): 0.190
Concentration (ug/L ): 5.088
Standard nunber 5 applied. [S.OOO]
Correlation coefficient: 0.99989 Slope: 0.0379
Hg2 ID: STD6:10.0ug/L Seq. No.: 0000? A/S Pos.: -- Date: 10/21/9'
Sample abs. is greater than that of the largest standard. v .
Reclicate 1 Tine: 10:1"
Peak Area (A-s): 8.952 ' Peak Height (A): 0.388
Blank Corrected Pk Height (A): 0.33E
Concentration (ug/L ): 10.231
Standard nunber 6 applied. [10.000]
Correlation coefficient: 0.99-5S9 Slooe: 0.0386
156
-------
ent File: HG..MEL Eleient: Hg2
: 10/21/97 ' Tine: 10:18
File: A6827.DAT 10/Wt File: A8827.IDW
nique: MHS Calib. Type: Linear
rk 1: STANDARDS: 3-023-5
Havelsngth: 253.7
Slit: 0.7 L
laup Current: 0
Energy: 71
M Display Calibration - C:\AAJSER\flflJILES\ELEMENT\HG_.MEL
0.388-,
B"
xx""x
^X^
x
jgf Linear
rgS S4 Corr. Coef.: B. 99989
C70o7s3 Slope: 8,8386
Pr~ Concentration 1B.BBB
4
5j
157
-------
Element File: H6..HEL Eleient: Hg2
Date: 10/21/97 . Tiie: 10:19
Data File: AB827.DAT I0/Ht File: A8827.IDW
Technique: MHS .Calib. Type: Linear
Renark 1: STANDARDS: 3-023-5
Renark 2: QC: 3-023-4.Ut
Wavelength: 253.7
Slit: 0.7 L
Laip Current: 0
Energy: 71
Hg2 ID: ICV:4.0ug/l
Seq. No.: 00010 A/S Pos.: -- Date: 10/21/97
Replicate 1 Tine: 10:21
Peak Area (A-s): 3.520 Peak Height (A): 0.152
Blank Corrected Pk Height (A): 0.152
Concentration (ug/L ): 3.941
Hg2 ID: ICB
Seq. No.: 00011 A/5 Pos.: - Date: 10/21/9'
Reolicate 1 Time: 10:23
Peak Area (A-s): 0.008 Peak Height (A): 0.000
Blank Corrected Pk Height (A): 0.000
Concentration (ug/L ): 0.005
Ha2 ID: CHECK LO
Seq. No.: 00012 A/S Pos.: -- Date: 10/21/9'
Reolicate 1 Time: 10:24
Peak Area (A-si: 0.163 Peak Height (A!: O.OOt
Blank Corrected Pk Height (A): 0.006
Concentration (ug/L ): 0.166
Hg2 ID: 43411 M82
Seq. No.: 00013 A/S Pos.: - Date: 10/21/9"
Reolicate 1 Time: 10:26
Peak Area (A-s): -0.003 Peak Height (Ai: 0.000
Blank Corrected Pk Height (A): 0.000
Concentration (ug/L ): 0.005
Hg2 ID: 43411 M82D
Seq. No.: 00014 A/S Pos.: - 'Date: 10/21/9'
Replicate 1 Tine: 10:27 '
Peak Area (A-s): -0.006 Peak Height (A): -0.000
Blank Corrected Pk Height (ft): -0.000
Concentration (ug/L ): -0.010
Replicate 1
Peak Area (A-s): 7.
s: 10:29 .
Peak Height .(ft): 0.321 ,
Blank Correci^trHeignt (A): 0.321
(ug/L ): 8.317
Hg2 ID: 43411 LCS2
Seq. No.: 00016 A/S Pos.: - Date: 10/21/9'
158
-------
icate I Ti»e: 10:36
Area (A-s).: 4.685 Peak Height (A): 0.205
(.Corrected Pk Height (A): 0.205
jntration (ug/L ): 5.325
ID: 43411 ICS2D
.cate 1
Area (A-s): 7.480
; Corrected Pk Height
intration
10: 43411 LCS20
Seq. No.: 00017 A/S Pos.: --
Seq. No.: 00013 A/S Pos.: -- Date: 10/21/9'
cate 1 Tine: 10:41
Area (A-s): 4.775 Peak Height (A): 0.211
, Corrected Pk Height (A): 0.211
.ntration (ug/L ): 5.473
ID: 184-34-6MS
-
Seq. No.: 00019 A/S Pos.: -- Date: 10/21/9"
cate 1 Time: 10:43
Area (A-s): 0.085 Peak Height (A): 0.003
Corrected Pk Height (A): 0.003
ntration (ug/L ): 0.081
MJC. *& it/-31-41 £C
ID: 184-84-6.Wftf D Seq. No.: 00020 A/S Pos.: -- Date: 10/21/9'
cate 1 Time: 10:44
Area (A-s): 0.07E Peak Height (A): 0.00!
Corrected Pk Height (A): 0.003
ntration (ug/L ): 0.075
ID: 184-84-6D
Seq. No.: 00021 A/S Pos.: - Date: 10/21/9'
cate 1 Time: 10:45
Area (A-s): 0.050 Peak Height (A): 0.002
Corrected Pk Height (A): 0.002
ntration (ug/L ): 0.044
ID: 184-84-6D D
Seq. No.: 00022 A/S Pos.: -- Date: 10/21/97
cate 1 Time: 10:46
Area iA-s): 0.042 Peak Height (A): 0.002
Corrected Pk Height (A): 0.002
ntration (ug/L ): 0.039
ID: 184-84-6D MS
Seq. No.: 00023 A/S Pos.: -- Date: 10/21/97
cate 1 Tiie: 10:47
Area (A-s): 7.446 Peak Height (A): 0.314
Corrected Pk Height (A): 0.3141
159
-------
/ . U . i f
Hg2 ID: 184-84-60 USD Seq. No.: 00024" A/S Pos.: •- Date: 10/21/97
Replicate 1 Tine: 10:49
Peak Area (A-s): 7.277 Peak Height (A): 0.306
Blank Corrected Pk Height (A): 0.306 ' _
Concentration (ug/L ): 7.947
Hg2 ID: CCV7:6.0ug/L Seq. No.: 00025 A/S Pos.: -- Date: 10/21/97
Replicate 1 Tine: 10:51
Peak Area (A-s): 5.168 Peak Height (A): 0.220
Blank Corrected Pk Height (A): 0.220
Concentration (ug/L ): 5.715
Hg2 ID: CCB Seq. No.: 00026 A/S Pos.: -- Oats: 10/21/9'
Reolicate 1 Tiie: 10:52
Peak Area (A-s): 0.026 Peak Height (A): 0.001
Blank Corrected Pk Height (A): 0.001
Concentration (ug/L i: 0.018
Hg2 ID: 134-84-6G Seq. No.: 00027 A/S Pos.: -- Date: 10/21/97
Replicate 1 Time: 10:53
Peak Area (A-s): 0.032 Peak Height (A): 0.001
Blank Corrected Pk Height (A): 0.001
Concentration (ug/L ): 0.034
i******!*!*!*,***,*, * *,**•,+, *,»,*, I**! tf^^*,^ ^ i,^*,,,*.*,^*. ,„*„+, t, ft *„ ti ^f.jv^tttf *,*, * I* a *••»*••• *•*•*•* •• I***** »* •*+,** ^tt*,^ m,*t I**,*,
Hg2 ID: 184-84-6G D Seq. No.: 00028 A/S Pos.: - Date: 10/21/9'
Replicate 1 Time: 10:55
Peak Area (A-s): -0.002 Peak Height (A): -0.000
Blank Corrected Pk Height (A): -0.000
Concentration (ug/L ): -0.003
*~*^**^^~^*****^^~***^***^^^*^**^-*ffi*'*ii,tf~,fr~,ft'*i*'**r-*'****r*r*f*i'***'*'tfi'*'*+t'it+,*t*,f,fitrt,^fr*,f,t,fm*,e,,
Hg2 ID: 184-84-6E Seq. He.: 00029 A/S Pos.: - Date: 10/21/97
Replicate I Tine: 10:56
Peak Area (A-s): 0.132 Peak Height (A): 0.005
Blank Corrected Pk Height (A): 0.005
Concentration (ug/L ): 0.138
Hg2 ID: 184-84-6E D
Seq. No.: 00030 A/S Pos.: -- Date: 10/21/97
Replicate 1 Tine: 10:56
Peak Area (A-s): 0.123 Peak Height (A): 0.005
Blank Corrected Pk Height (A): 0.005
Concentration (ug/L ): 0.127
160
-------
• 10: 184-84-6F
Seq. No.: 00031 A/S Pos.: -- Date: 10/21/97
licate 1 Ti«e: 10:57
k Area (A-s): 0.001 Peak Height (A): -0.000
nk Corrected Pk Height (A): -0.000
:entration (ug/L ): -0.003
ID: 184-84-6F 0 Seq. No.: 00032 A/S Pos.: -- Date: 10/21/9'
.icate 1 Tine: 10:59
: Area (A-s): 0.002 Peak Height (A): 0:000
ik Corrected Pk Height (A): 0.000
isntration (ug/L ): 0.003
Wo
ID: 184-84-7WA8- _ Seq. No.: 00033 A/S Pos.: - Date: 10/21/97
. ^VU,.,,x,n fcc
icate 1 - Tine: 11:00
Area (A-s):- 0.030 Peak Height (A): 0.001
k Corrected Pk Height (A): 0.001
entration (ug/L ): 0.031
•*> it-swi tt
ID: 1S4-84-7CWB D Seq. No.: 00034 A/S Pos.: -- Date: 10/21/9'
icate 1 Time: 11:01
Area (A-s): 0.025 Peak Height (A): 0.001
k Corrected Pk Height (A): 0.001
entration (ug/L ): 0.018
10: 184-84-7G Sea. No.: 00035 A/S Pos.: -- Date: 10/21/97
icate 1 Time: 11:02
Area (A-s): -0.005 Peak Height (A): 0.000
k Corrected Pk Height (A): 0.000
Entration (ug/L ): 0.000
ID: 184-84-7G D Seq. No.: 00036 A/S Pos.: -- Date: 10/21/9'
icate 1 Time: 11:05
Area (A-s): -0.024 Peak Height (A): -0.001
< Corrected Pk Height (A): -0.001
sntration (ug/L ): -0.018
ID: CCV8:6.0ug/L Seq. No.: 00037 A/S Pos.: - Date: 10/21/97
.cate 1 Tine: 11:06
Area (A-s): 4..679 Peak Height (A): 0.200
Corrected Pk Height (A): 0.200
ntration (ug/L ): 5.187
ID: CCB
Seq. No.: 00038 A/S Pos.: -- - Date: 10/21/97
161
-------
Peak .Area (A-s): 0.027 Peak Height (A): 0.001*
Blank Corrected.Pk Height (A): 0.001
Concentration (ug/L ): 0.021
Hg2 ID: 184-84-7EF Seq. Ho.: 00039 A/S Pos.: -- Date: 10/21/9'
Replicate 1 • Time: 12:21
Peak Area (A-s): 0.046 Peak Height (A): 0.002
Blank Corrected Pk Height (A): 0.002
Concentration (ug/L ): 0.044
Hg2 ID: 184-84-7EF 0 Seq. No.: 00040 A/S Pos.: -- Date: 10/21/9'
Replicate 1 Tine: 12:22
Peak Area (A-s): 0.039 Peak Height (A): 0.001
Blank Corrected Pk Height (A): 0.001
Concentration (ug/L ): 0.036
Hg2 ID: 184-S4-7EF HS Seq. No.: 00041 A/S Pos.: -- Date: 10/21/9'
Replicate I Time: 12:23
Peak Area (A-s): 7.762 Peak Height (A): 0.326
Blank Corrected Pk Height (A): 0.326
Concentration (ug/L ): 8.442
Hg2 10: 134-84-7EF USD See. No.: 00042 A/S Pos.: - Date: 10/21/9'
Reolicate 1 Tine: 12:24
Peak Area (A-s!: 7.774 Peak Height (A): 0.331
Blank Corrected Pk Height (A): 0.331
Concentration (ug/L ): 8.587
Hg2 ID: 184-84-7H Ssq. No.: 00043 A/S Pos.: - Date: 10/21/97
Replicate 1 Time: 12:25
Peak Area (A-s): 0.141 Peak Height (A): 0.006
Blank Corrected Pk Height (A): 0.006
Concentration (ug/L ); 0.148
Hg2 ID: 184-84-7H D Seq. No.: 00044 A/5 Pos.: - Date: 10/21/9'
Replicate 1 Tine: 12:26
Peak Area (A-s): 0.108 Peak Height (A): 0.004
Blank Corrected Pk Height (A): 0.004
Concentration (ug/L ): 0.112
Hg2 ID: 184-34-71
Seq. No.: 00045 A/S Pos.: - Date: 10/21/9*
Replicate 1 • Tine: 12:27
Peak Area (A-s): 0.009 Peak Height (A): 0.000
Blank Corrected Pk Height (A): 0.000
162
-------
2 10: 184-84-71 D Seq. No.: 00046 A/S Pos.: - Date: 10/21/97
olicate 1 Tine: 12:28
ak Area (A-s): 0.004 Peak Height (A): 0.000
ank Corrected Pk Height (A): O.OOiX
ncentration (ug/L ): 0.003
I ID: CCV9:6.0ug/L Seq. No.: 00047 A/S Pos.: -- Date: 10/21/97
jlicate 1 Tine: 12:29
ik Area (A-s): 5.101 Peak Height (A): 0.216
ink Corrected Pk Height (A): Or216
icentration (ug/L ): 5.609
! ID: CC8 " Seq. No.: 00048 A/S Pos.: - Date: 10/21/9'
ilicate 1 Time: 12:33
ik Area (A-s): -0.011 Peak Height (A): -0.00!
ink Corrected Pk Height (A): -0.001
icentration (ug/L ): -0.013
! ID: 43377 HB1 Seq. No.: 00049 A/S Pos.: -- Date: 10/21/9"
ilicate I lime: 12:34
ik Area (A-si: -0.005 Peak Height (At: -0.000
ink Corrected Pk Height (A): -0.000
icsntration (ug/L ): -O.OOS
! ID: 43377 HB1 D Seq. No.: 00050 A/S Pos.: - Date: 10/21/9'
ilicate 1 Time: 12:35
ik Area (A-s): -0.011 Peak Height (A): -0.001
ink Corrected Pk Height (A): -0.001
icentration (ug/L ): -0.016
! ID: 43377 LCS1 Seq. No.: 00051 A/5 Po<_*—*"^Date: 10/21/9
ilicate 1 ^^^-^Tj«e:12:36
ik Area (A-s): 7.457^^-^"^ Peak Height (A): 0.322
ink CorrectedJlMslght (A): 0.322
icentratierTT^g/L ): 8.340
' ID: 43377 LCS1 Seq. No.: 00052 A/S Pos.: - Date: 10/21/9'
•licate 1 • Tine: 12:41
k Area (A-s): 4.712 Peak Height (A): 0.204
nk Corrected Pk Height (A): 0.204
centration (ug/L ): 5.278
163
-------
ID/Height File: A8828.IDN Analyst: D.STREETER-EDHARDS
Saiple Volute: 100 iL Noiinal Height: 1.0 g
Loc. Saiple ID Height Dilution
0
1
2
3
4
5
6
7
8
9
10
11
12
13
14
15
16
17
18
19
20
21
22
23
24
25
26
27
28
29
30
31
32
33
34
35
36
37
38
39
40
41
42
43
44
45
46
47
48
49
50
isr
1?
13
ST BLANK "X
STDl=0.2ug/L \
STD2=0.5ug/L /
STD3=1.0ug/L (
STD4--2.0ug/L 7-
STD5:5.0ug/L (
STD6=10.0ug/L 1
ICV:4.0ug/L ^__
IC8
CHECK LO
43377 MB2
43377 MB2D
43377 LCS
45377 LCSt-
184-50-6B
184-50-68 D
184-50-680
184-50-6BO 0
184-50-680 MS
184-50-6BD MSD
CCV7--6.0ug/L
CCB
184-50-6E
184-50-6E 0
184-50-6FE
184-50-6FE D
184-50-7CA8
184-50-7CAB D
184-50-7E
184-50-7E 0
184-50-7F
.184-50-7F D
CCV8:6.0ug/l
CCB
184-50-70
184-50-7D 0
184-50-70 MS
184-50-70 MSO
CCV9:6.0ug/L
CCB
42011 Cnl MB
42011 Cnl MSO
42011 LCS
42011 LCSD
170-70-3
170-70-3 D
170-70-3 MS
170-70-3 HSD
CCV:6.0ug/L
CCB
43411 MB3
43411 MB 3 D
43411 LCS3
43411 LCS30
3 - 0 93-*? &5£
-3-0a3-r P^
•3-oa3-? ^E
3 -0^3- £* &5tr
3-0>53-ff |Q£ jo
- 3-Cbi3^ £5c
-------
)C.
i'i
isl
)6l
H"'
'8"'.
,0"
.1 '
,2
,3
>4
,5
6
,7
Saaple ID Height Dilution
184-84-580
184-84-5BD 0
184-84-580 HS
184-84-580 USD
CCV10=6.0ug/l —3-023-8 fcS
CCB
184-84-5E
184-84-5E D
184-84-5F
184-84-5F D
184-84-5GF
184-84-5GF D -^
CCVll:6.0ug/L -3-^^"^
CCB
165
-------
Eleaent File: H6..MEL
Eleient: Hg2
Print Data: Hain+Suppl.
Print: Calib. Curve
Reiarks:
STANDARDS: 3-023-7
QC: 3-023-8
INSTRUMENT: 5100
Wavelength: 253.7 Peak
Signal Type: AA
Read Tine: 30.0
Satple Replicates: 1
Standard Replicates: 1
FLAME:
Flame Type: Air
Oxidant Flow: 10.0 L/nin
Calibration Type: Linear
QC:
Matrix Check Calculations:
\ Difference for Dupls: No
* Recovery for Spike: No
Analyst: D STREETER-EDHARDS
Peak Storage: None
Technique: MHS Version: 7.01
Slit: 0.7 Lou
Signal Measureaent: Peak Height (5)
Read Delay: 1.0 BOC Tiie: 2
Flame Sensor: On
Fuel Flow: 2.0 L/ain
CALIBRATION:
Solutions
^.I;L B 1 .» « L
taiiu. dianK
Standard 1
Standard 2
Standard 3
Standard 4
Standard 5
Standard 6
Calibration
i ID
1
1
1 CTf\ ft I V
,5IU OLft
ISTD i
ISTD 2
ISTD 3
ISTD 4
ISTD 5
ISTD 6
Units: ug/L
Cone |
t
(
....... - 1
I
0.2001
0.500!
1.000|
2.000|
5.0001
10.0001
Sanple Units:
ug/L
Locations:
Locations:
Cone:
166
-------
«ent File: H6..HEL Eleient: Hg2
B: 10/22/97 Tiie: 09:46
a File: AB828.DAT ID/Nt File: AB828.IDH
hnique: HHS Calib. Type: Linear
ark 1: STANDARDS: 3-023-7
ark 2: QC: 3-023-8
Wavelength: 253.7
Slit: 0.7 L
Laip Current: 0
Energy: 71
10: Seq. 00001
icate 1
; Area (A-s): 0.290
ik Corrected Pk Height (A): 0.012
i-zero perforaed.
Seq. Ho.: 00001 A/S Pos.: - Date: 10/22/97
Ti»e: 09:46
Peak Height (A): 0.012
Seq. No.: 00002 A/S Pos.: -- Date: 10/22/9^
ID: Seq. 00002
icate 1
Area (A-s): 0.020
ik Corrected Pk Height (A): 0.001
-zero performed.
Time: 09:47
Peak Height (A): 0.001
167
-------
Elenent File: HG..MEL Eleient: Hg2
Date: 10/22/97 Tiie: 09:48
Data File: AB823.DAT ID/Ht File: AB823.IDH
Technique: HHS Calib. Type: Linear
Reiark 1: STANDARDS: 3-023-7
Reiark 2: QC= 3-023-8
Wavelength: 253.7
Slit: 0.7 I
Laip Current: 0
Energy: 71
Hg2 10: ST BLANK
Seq. Ho,: 00003 A/S Pos.: -- Date: 10/22/97
Replicate 1 Tiie: 09:50
Peak Area (A-s): -0.000 Peak Height (A): -0.000
Blank Corrected Pk Height (A): -0.000
Auto-zero perforaed.
Hg2 ID: STDl:0.2ug/L
Seq. No.: 00004 A/S Pos.: -- Date: 10/22/9'
Replicate 1 Time: 09:52
Peak Area (A-s): 0.162 Peak Height (A): 0.00'
Blank Corrected Pk Height (A): 0.007
Standard number 1 applied. [0.200]
Correlation coefficient: 1.00000 Slope: 0.0331
Hg2 10: ST02:0.5ug/L
Seq. No.: 00005 A/S Pos.: -- Date: 10/22/97
Sample abs. is greater than that of the largest standard.
Replicate 1 Tine: 09:53
Peak Area (A-s): 0.429 Peak Height (A): 0.018^ -.*
Blank Corrected Pk Height (A): 0.018 .s^ Xv &
Concentration (ug/L ): 0.548 ^
Hg2 ID: STD3:1.0ug/L
Sasple abs. is greater ttj^rThat of the largest standard.
Replicate 1 ^^ Tine: 09:54
Peak Area (A-s)xO86 Peak Height (A): 0.038
Blank Correefed Pk Height (A): 0.038
ConcejiKeftion (ug/L ): 1.145
Hg2 ID: STD2=0.5ug/L Seq. No.: 00007 A/S Pos.: -- Date: 10/22/97
Sample abs. is greater than that of the largest standard.
Replicate 1 Tiie: 10:01
Peak Area (A-s): 0.470 Peak Height (A): 0.021
Blank Corrected Pk Height (ft): 0.021
Concentration (ug/L ): 0.621
Standard nuiber 2 applied. [0.500]
Correlation coefficient: 0.98455 Slope: 0.0402
168
-------
ID: ST03:1.0ug/L
Seq. Ho.: 00008 A/S Pos.: - Date: 10/22/97
pie abs. is greater than that of the largest standard.
licate 1 Tue: 10:02
k Area (A-s): 0.913 Peak Height (A): 0.041
nk Corrected Pk Height (A): 0.041
centration (ug/L ): 1.020
ndard nuiber 3 applied. [1.000]
relation coefficient: 0.99775 Slope: 0.0409
ID: STD4:2.0ug/L
Seq. No.: 00009 A/S Pos.: - Date: 10/22/97
pie abs. is greater than that of the largest standard.
licate 1 Tine: 10:03
k Area (A-s): 1.700 Peak Height (A): 0.073
nk Corrected Pk Height (A): 0.073
centration (ug/L ): 1.798
ndard number 4 applied. [2.000]
relation coefficient: 0.99647 Slope: 0.0378
ID: STD5:5.0ug/l
Seq. No.: 00010 A/S Pos.: -- Date: 10/22/97
t>le abs. is greater than that of the largest standard.
licate 1 Time: 10:05
k Area (A-s): 4.214 Peak Height (A): 0.180
nk Corrected Pk Height (A): 0.180
:entration (ug/L ): 4.768
ndard number 5 applied. [5.000]
relation coefficient: 0.99923 Slope: 0.0364
ID: STD6:10.0ug/L Seq. No.: 00011 A/S Pos.: - Date: 10/22/9-
Die abs. is greater than that of the largest standard.
licate 1 Tine: 10:06
k Area (A-s): 8.381 Peak Height (A): 0.363
nk Corrected Pk Height (A): 0.363
:entration (ug/L ): 9.993
idard number 6 applied. [10.000]
relation coefficient: 0.99984 Slope: 0.0364
169
-------
Eleient File: HG..HEL Eleient: Hg2
Date: 10/22/97 Tiie: 10:07
Data File: AB828.DAT ID/Ht File: AB828.IDH
Technique: HHS Calib. Type: Linear
Reiark 1: STANDARDS: 3-023-7
ReBark 2: QC: 3-023-8
Wavelength: 253.7
Slit: 0.7 L
Laip Current: 0
Energy: 71
H| Display Calibration - C;\flfl_USER\flfl.FILES\ELEHEHT\H6_.HEL
Linear
Corn. Coef.: 8.99984
Slope; B.Q364
Concentration
18.
170
-------
ID: ICV:4.0ug/l Seq. No.: 00012 A/S Pos.: - Date: 10/22/97
licate 1 Tiie: 10:12
< Area (A-s): 3.522 Peak Height (A): 0.150
ik Corrected Pk Height (A): 0.150
:entration (ug/L ): 4.137
ID: ICB Seq. No.: 00013 A/S Pos.: - Date: 10/22/97
.icate 1 Tise: 10:13
; Area (A-s): 0.014 Peak Height (A): 0.000
ik Corrected Pk Height (A): 0.000
:entration (ug/L ): 0.003
ID: CHECK LO Seq. No.: 00014 A/S Pos.: -- Date: 10/22/97
icate 1 Tine: 10:15
. Area (A-s): 0.173 Peak Height (A): 0.007
ik Corrected Pk Height (A): 0.007
lentration (ug/L ): 0.199
ID: 43377 MB2 Seq. No.: 00015 A/S Pos.: -- Date: 10/22/9'
icate 1 Tiie: 10:18
. Area (A-s): 0.003 Peak Height (A): 0.000
ik Corrected Pk Height (A): 0.000
entration (ug/L ): 0.003
ID: 43377 MB2D Seq. No.: 00016 A/S Pos.: - Date: 10/22/97
icate 1 Tine: 10:19
Area (A-s): 0.005 Peak Height (A): -0.000
ik Corrected Pk Height (A): -0.000
entration (ug/L ): -0.003
ID: 43377 LCS Seq. No.: 00017 A/S Pos.: - Date: 10/22/9'
icate I Tine: 10:20
Area (A-s): 4.228 Peak Height (A): 0.181
k Corrected Pk Height (A): 0.181
entration (ug/L ): 4.981
ID: 43377 LCSD Seq. No.: 00018 A/S Pos.: -- Date: 10/22/97
icate 1 Tiie: 10:22
Area (A-s): 4.003 Peak Height (A): 0.172
k Corrected Pk Height (A): 0.172
entration (ug/L ): 4.733
ID: 184-50-68
Seq. Ho.: 00019 A/S Pos.: -- Date: 10/22/97
171
-------
Concentration {ug/L ): 4.948
Hg2 ID: 170-70-3 Seq. No.: 00049 A/S Pos.: - Date: 10/22/97
Replicate 1 Tiie: 10:57
Peak Area (A-s): 0.042 Peak Height (A): 0.002
Blank Corrected Pk Height (ft): 0.002
Concentration (ug/L ): 0.041
Hg2 ID: 170-70-3 D Seq. No.: 00050 A/S Pos.: - Date: 10/22/97
Replicate 1 Tine: 10:59
Peak Area (A-s): 0.036 Peak Height (A): 0.002
Blank Corrected Pk Height (A): 0.002
Concentration (ug/L ): 0.041
Hg2 ID: 170-70-3 MS Seq. No.: 00051 A/S Pos.: - Date: 10/22/9'
Replicate 1 Time: 11:00
Peak Area (A-s): 3.664 Peak Height (A): 0.16?
Blank Corrected Pk Height (ft): 0.169
Concentration (ug/L ): 4.65S,
Hg2 ID: 170-70-3 MSD Seq. No.: 00052 A/S Pos.: -- Date: 10:22''9'
Replicate 1 Time: 11:01
Peak Area (A-s.l: 3.993 Peak Height (A): 0.1S2
Blank Corrected Pk Height (A): 0.182
Concentration (ug/L ): 5.020
Hg2 ID: CCV=6.0ug/L Sea. No.: 00053 A/S Pos.: -- Date: 10/22/97
Reolicate 1 Tine: 11:02
Peak Area (A-s): 4.793 Peak Height (A): 0.228
Blank Corrected Pk Height (A): 0.228
Concentration (ug/L ): 6.278
Hg2 ID: CCB Seq. No.: 00054 A/S Pos.: -- Date: 10/22/9*
Replicate 1 Time: 11:04
Peak Area (A-s): 0.039 Peak Height (A): 0.002
Blank Corrected Pk Height (A): 0.002
Concentration (ug/L ): 0.044
Hg2 ID: 43411 HB3
Seq. No.: 00055 A/S Pos.: - Date: 10/22/9*
Replicate 1 Tine: 11:05
Peak Area (A-s): 0.036 Peak Height (A): 0.001
Blank Corrected Pk Height (A): 0.001
Concentration (ug/L ): 0.036
172
-------
10: 43411 M83 D Seq. No.: 00056 A/S Pos.: - Date: 10/22/97
icate 1 Tiie: 11:07
Area (A-s): 0.028 Peak Height (A): 0.001
k Corrected Pk Height (A): 0.001
entration (ug/L ): 0.022
ID: 43411 LCS3 Seq. No.: 00057 A/S Pos.: - Date: 10/22/97
icate 1 Ti«e: 11:08
Area (A-s): 3.908 Peak Height (A): 0.182
k Corrected Pk Height (A): 0.182
sntration (ug/L ): 5.001
ID: 43411 LCS3D Seq. No.: 00058 A/S Pos.: -- Date: 10/22/97
icate 1 Time: 11:09
Area (A-s): 3.165 Peak Height (A): 0.176
< Corrected Pk Height (A): 0.176
;ntration (ug/L ): 4.846
ID: 184-34-5BD Seq. No.: 00059 A/S Pos.: - Date: 10/22/9'
icate 1 Time: 11:10
Area (A-s): 0.050 Peak Height (A): 0.002
< Corrected Pk Height (A): 0.002
:ntration (ug/L ): 0.050
ID: 184-84-5BD D Seq. No.: 00060 A/S Pos.: -- Date: 10/22/97
icate 1 Time: 11:11
Area (A-s): 0.028 Peak Height (A): 0.001
< Corrected Pk Height (A): 0.001
;ntration (ug/L ): 0.033
ID: 184-84-5BD MS Seq. No.: 00061 A/S Pos.: -- Date: 10/22/97
:cate 1 Tine: 11:11
Area (A-s): 4.042 Peak Height (A): 0.179
( Corrected Pk Height (A): 0.179
miration (ug/L ): 4.926
ID: 184-84-5BD HSD Seq. No.: 00062 ft/S Pos.: -- Date: 10/22/97
cate 1 Tine: 11:12
Area (A-s): 3.862 Peak Height (A): 0.185
Corrected Pk Height (A): 0.185
ntration (ug/L ): 5.092
ID: CCV10:6.0ug/L Seq. No.: 00063 A/S Pos.: - Date: 10/22/97
173
-------
Replicate 1 Tiie: 11:13
Peak Area (A-s): 5.201 Peak Height (A): 0.246
Blank Corrected Pk Height (A): 0.246
Concentration (ug/L ): 6.775
Hg2 ID: CCB Seq. No.: 00064 A/S Pos.: - Date: 10/22/97
Replicate 1 Tine: 11:14
Peak Area (A-s): 0.075 Peak Height (A): 0.003
Blank Corrected Pk Height (A): 0.003
Concentration (ug/L ): 0.080
Hg2 ID: 184-84-5E Seq. No.: 00065 A/S Pos.: -- Date: 10/22/97
Replicate 1 Tine: 11:15
Peak Area (A-s): 0.043 Peak Height (A): 0.002
Blank Corrected Pk Height (A): 0.002
Concentration (ug/L ): 0.041
Hg2 ID: 184-84-5E D Seq. No.: 00066 A/S Pos.: - Date: 10/22/97
Replicate 1 Tine: 11:16
Peak Area (A-s): 0.033 Peak Height (A): 0.001
Blank Corrected Pk Height (A): 0.001
Concentration (ug/L ): 0.036
Hg2 ID: 184-84-5F Seq. No.: 00067 A/S Pos.: -- Date: 10/22/97
Replicate 1 Tine: 11:16
Peak Area (A-s): 0.033 Peak Height (A): 0.001
Blank Corrected Pk Height (A): 0.001
Concentration (ug/L ): 0.030
Hg2 ID: 184-84-5F D Seq. No.: 00068 A/S Pos.: - Date: 10/22/97
Replicate 1 Time: 11:17
Peak Area (A-s): 0.030 Peak Height (A): 0.001
Blank Corrected Pk Height (A): 0.001
Concentration (ug/L ): 0.025
Hg2 ID: 184-84-5GF Seq. No.: 00069 A/S Pos.: -- Date: 10/22/97
Replicate 1 Tine: 11:18
Peak Area (A-s): 0.045 Peak Height (A): 0.002
Blank Corrected Pk Height (A): 0.002
Concentration (ug/L ): 0.044
Hg2 ID: 184-84-56F D
Seq. No.: 00070 A/S Pos.: -- Date: 10/22/97
Replicate 1 Tine: 11:19
Peak Area (A-s): 0.043 Peak Height (A): 0.002
Blank Corrected Pk Height (A): 0.002
174
-------
ncentration (ug/L ): 0.041
2 10: CCVll:6.0ug/L Seq. Ho.: 00071 A/S Pos.: -- Date: 10/22/97
plicate 1 Tiie: 11:19
ak Area (A-s): 4.696 Peak Height (A): 0.236
ank Corrected Pk Height (A): 0.236
ncentration (ug/L ): 6.485
2 ID: CCB Seq. Ho.: 00072 A/'S Pos.: - Date: 10/22/97
Dlicate 1 Tine: 11:20
ak Area (A-s): 0.046 Peak Height (A): 0.002
ank Corrected Pk Height (A): 0.002
ncentration (ug/L ): 0.047
175
-------
-------
APPENDIX D
COMPUTER SUMMARIES
-------
Appendix D.I
Computer Summaries
Baghouse Inlet - Method 23 & 29
-------
Summary of Stack Gas Parameters and Test Results
As-pHfH-TVt-Atrr "8" - Gary, North Carolina
US EPA Test Method 23 - PCDD / PCDF
Baghouse Inlet
Page 1 of 6
Y
AH
Pbar
vm
Tm
Pstatic
Ts
vte
CO2
02
N2
CP
Ap1*
e
Dn
An
Vm(std)
Vm(sld)
PS
Bw,
Vwstd
1-B™
Md
Ms
Vs
A
Qa
Q.
Qs(cmm)
I
RUN NUMBER
RUN DATE
RUN TIME
MEASURED DATA
Meter Box Correction Factor
Avg Meter Orifice Pressure, in. H2O
Barometric Pressure, inches Hg
Sample Volume, ft3
Average Meter Temperature, °F
Stack Static Pressure, inches H2O
Average Stack Temperature, °F
Condensate Collected, ml
Carbon Dioxide content, % by volume
Oxygen content, % by volume
Nitrogen content, % by volume
Pilot Tube Coefficient
Average Square Root Dp, (in. H2O)iy2
Sample Run Duration, minutes
Nozzle Diameter, inches
CALCULATED DATA
Nozzle Area, ft2
Standard Meter Volume, dscf
Standard Meter Volume, dscm
Stack Pressure, inches Hg
Moisture, % by volume
Standard Water Vapor Volume, ft3
Dry Mole Fraction
Molecular Weight (d.b.), Ib/lb-mole
Molecular Weight (w.b.), Ib/lb-mole
Stack Gas Velocity, ft/s
Stack Area, ft2
Stack Gas Volumetric flow, acfm
Stack Gas Volumetric flow, dscfm
Stack Gas Volumetric flow, dscmm
Isokinetic Sampling Ratio, %
R-M23-I-1
8/27/97
0940-1227
1.021
1.21
29.80
58.263
96
-1.8
308
510.5
5.2
13.8
81.0
0.84
0.6901
96
0.257
0.00036
56.399
1.597
29.67
29.9
24.029
0.701
29.38
25.98
49.5
16.20
48,074
22,981
650.7
115.0
R-M234-2
8/28/97
0908-1428
1.021
0.286
29.60
53.015
96
-1.8
306
414.9
5.2
13.1
81.7
0.84
0.6755
170
0.194
0.00021
50.885
1.441
29.47
27.7
19.529
0.723
29.36
26.21
48.3
16.20
46,957
23,027
652.1
102.6
R-M23-I-3
8/29/37
0818-1413
1.021
0.396
29.60
83.709
93
-1.8
290
393.0
4.0
15.2
80.8
0.84
0.7133
240
0.194
0.00021
80.735
2.286
29.47
18.6
18.499
0.814
29.25
27.15
49.6
16.20
48,211
27,178
769.6
97.7
Average of
1st and 2nd
Test Run
1.021
0.75
29.70
55.639
96
-1.8
307
462.7
5.2
13.5
81.4
0.84
0.6828
133
0.226
0.00028
53.642
1.519
29.57
28.8
21.779
0.712
29.37
26.09
48.9
16.20
47,515
23,004
651.4
108.8
-------
Summary of Stack Gas Parameters and Test Results
foptttu- 7*Aur"«" • Gary, North Carolina
US EPA Test Method 23 - PCDD / PCDF
Baghouse Inlet
Page 2 of 6
(ng)
(ng/dscm)
(M9/hr)
(ng)
(ng/dscm)
(pg/hr)
(ng)
(ng/dscm)
(pg/hr)
(ng)
(ng/dscm)
(pg/hr)
(ng)
(ng/dscm)
(pg/hr)
(ng)
(ng/dscm)
(pg/hr)
RUN NUMBER
RUN DATE
RUN TIME
EMISSIONS DATA
DIOXINS:
2378 TCDD
Catch, ng
Concentration, ng/dscm, as measured
Emission Rate, pg/hr
Total TCDD
Catch, ng
Concentration, ng/dscm, as measured
Emission Rate, pg/hr
12379PeCPP
Catch, ng
Concentration, ng/dscm, as measured
Emission Rate, pg/hr
Total PeCDD
Catch, ng
Concentration, ng/dscm, as measured
Emission Rate, pg/hr
123478 HxCDD
Catch, ng
Concentration, ng/dscm, as measured
Emission Rate, pg/hr
123678 HxCDD
Catch, ng
Concentration, ng/dscm, as measured
Emission Rate, pg/hr
R-M23-I-1
8/27/97
0940-1227
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
R-M23-I-2
8/28/97
0908-1428
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
R-M23-I-3
8/29/97
0818-1413
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
Avenge of
1st and 2nd
Test run
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
() Not Detected. Value shown is the detection limit for that sample.
{} Estimated Maximum Possible Concentration.
-------
Summary of Stack Gas Parameters and
Test Results
.?:?*4tr TiAm "g"i - Gary, North Carolina
US EPA Test Method 23 - PCDO / PCDF
RUN NUMBER
RUN DATE
RUN TIME
Baghouse Inlet
Page 3 of 6
R-M23-I-1
8/27/97
0940-1227
R-M23-I-2
8/28/97
0908-1428
R-M23-I-3
8/29/97
0818-1413
Avenge of
1st and 2nd
Test Run
EMISSIONS DATA -Continued
(ng)
(ng/dscm)
(pg/hr)
(ng)
(ng/dscm)
(pg/hr)
(ng)
(ng/dscm)
(pg/hr)
(ng)
(ng/dscm)
(pg/hr)
(ng)
(ng/dscm)
(pg/hr)
(ng)
(ng/dscm)
(pg/hr)
DIOXINS - Continued
123789 HxCDD
Catch, ng
Concentration, ng/dscm,
Emission Rate, pg/hr
Total HxCDD
Catch, ng
Concentration, ng/dscm,
Emission Rate, pg/hr
1234678 HpCDD
Catch, ng
Concentration, ng/dscm,
Emission Rate, pg/hr
Total HpCDD
Catch, ng
Concentration, ng/dscm,
Emission Rate, pg/hr
1 2346789 OCPD
Catch, ng
Concentration, ng/dscm,
Emission Rate, pg/hr
Total PCDD
Catch, ng
Concentration, ng/dscm,
Emission Rate, pg/hr
ND
as measured ND
ND
ND
as measured ND
ND
ND
as measured ND
ND
{0.350}
as measured {0.219}
{8.56}
9.70
as measured 6.07
237
{10.1}
as measured {6.29}
{246}
-
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
8.20
5.69
223
8.20
5.69
223
ND
ND
ND
0.0200
0.00875
0.404
0.140
0.0612
2.83
0.340
0.149
6.87
16.2
7.09
327
16.6
7.24
334
ND
ND
ND
ND
ND
ND
ND
ND
ND
{0.175}
{0.110}
{4.28}
8.95
5.88
230
{9.13}
{5.99}
{234}
() Not Detected. Value shown is the detection limit for that sample.
{} Estimated Maximum Possible Concentration.
-------
Summary of Stack Gas Parameters and
Test Results
fcpHter Tt/fcur "B '•'- Gary, North Carolina
US EPA Test Method 23 - PCDD /
RUN NUMBER
RUN DATE
RUN TIME
Baghouse Inlet
Page 4 of 6
R-M23-I-1
8/27/97
0940-1227
PCDF
R-M23-I-2
8/28/97
0908-1428
R-M23-I-3
8/29/97
0818-1413
Average of
1st and 2nd
Test Run
EMISSIONS DATA - Continued
(ng)
(ng/dscm)
(ug/hr)
(ng)
(ng/dscm)
(ug/hr)
(ng)
(ng/dscm)
(ug/hr)
(ng)
(ng/dscm)
(ug/hr)
(ng)
(ng/dscm)
(ug/hr)
(ng)
(ng/dscm)
(ug/hr)
FURANS
2378 TCDF
Catch, ng
Concentration, ng/dscm,
Emission Rate, ug/hr
Total TCDF
Catch, ng
Concentration, ng/dscm,
Emission Rate, ug/hr
12378 PeCDF
Catch, ng
Concentration, ng/dscm,
Emission Rate, ug/hr
23478 PeCDF
Catch, ng
Concentration, ng/dscm,
Emission Rate, ug/hr
Total PeCDF
Catch, ng
Concentration, ng/dscm
Emission Rate, ug/hr
1 23478 HxCDF
Catch, ng
Concentration, ng/dscm
Emission Rate, ug/hr
ND
as measured ND
ND
{0.180}
as measured {0.113}
{4.40}
ND
as measured ND
ND
ND
as measured ND
ND
0.470
as measured 0.294
11.5
ND
as measured ND
ND
ND
ND
ND
0.170
0.118
4.62
ND
ND
ND
ND
ND
ND
0.330
0.229
8.96
ND
ND
ND
ND
ND
ND
0.0100
0.00437
0.202
ND
ND
ND
ND
ND
ND
{0.0100}
{0.00437}
{0.202}
0.0200
0.00875
0.404
ND
ND
ND
{0.175}
{0.115}
{4.51}
ND
ND
ND
ND
ND
ND
0.400
0.262
10.2
ND
ND
ND
() Not Detected. Value shown is the detection limit for that sample.
{} Estimated Maximum Possible Concentration.
-------
ftspnAtrTiAMT "B" - Gary, North Carolina
US EPA Test Method 23 - PCDD / PCDF
Baghouse Inlet
(ng)
(ng/dscm)
(pg/hr)
(ng)
(ng/dscm)
(pg/hr)
(ng)
(ng/dscm)
(pg/hr)
(ng)
(ng/dscm)
(pg/hr)
(ng)
(ng/dscm)
(pg/hr)
(ng)
(ng/dscm)
(|jg/hr)
Page
RUN NUMBER
RUN DATE
RUN TIME
EMISSIONS DATA - Continued
Furans - Continued
123678 HxCDF
Catch, ng
Concentration, ng/dscm, as measured
Emission Rate, pg/hr
234678 HxCDF
Catch, ng
Concentration, ng/dscm, as measured
Emission Rate, pg/hr
123789 HxCDF
Catch, ng
Concentration, ng/dscm, as measured
Emission Rate, pg/hr
Total HxCDF
Catch, ng
Concentration, ng/dscm, as measured
Emission Rate, pg/hr
1 234678 HpCDF
Catch, ng
Concentration, ng/dscm, as measured
Emission Rate, pg/hr
1234789 HpCDF
Catch, ng
Concentration, ng/dscm, as measured
Emission Rate, pg/hr
5 of 6
R-M23-I-1
8/27/97
0340-1227
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
R-M23-I-2
8/28/97
0908-1428
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
. ND
ND
ND
ND
ND
ND
ND
ND
R-M23-I-3
8/29/97
0818-1413
ND
ND
ND
{0.00600}
{0.00262}
{0.121}
ND
ND
ND
0.0300
0.0131
0.606
0.0400
0.0175
0.808
ND
ND
ND
Average of
1st and 2nd
Test run
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
() Not Detected. Value shown is the detection limit for that sample.
{} Estimated Maximum Possible Concentration.
-------
Summary of Stack Gas Parameters and Test Results
A&H&.T TLA™ "8" , - Gary, North Carolina
US EPA Test Method 23 - PCDD / PCDF
Baghouse Inlet
Page 6 of 6
(ng)
(ng/dscm)
(pg/hr)
(ng)
(ng/dscm)
(pg/hr)
(ng)
(ng/dscm)
(pg/hr)
(ng)
(ng/dscm)
(pg/hr)
RUN NUMBER
RUN DATE
RUN TIME
EMISSIONS DATA - Continued
Furans - Continued
Total HpCDF
Catch, ng
Concentration, ng/dscm, as measured
Emission Rate, (jg/hr
1 2346789 OCDF
Catch, ng
Concentration, ng/dscm, as measured
Emission Rate, pg/hr
Total PCDF
Catch, ng
Concentration, ng/dscm, as measured
Emission Rate, pg/hr
Total PCDD + PCDF
Catch, ng
Concentration, ng/dscm, as measured
Emission Rate, pg/hr
R-M23-I-1
8/27/97
0940-1227
ND
ND
ND
ND
ND
ND
{0.650}
{0.407}
{15.9}
{10.7}
{6.70}
{262}
R-M23-I-2
8/28M7
0908-1428
{0.260}
{0.180}
{7.06}
ND
ND
ND
{0.760}
{0.527}
{20.6}
{8.96}
{6.22}
{243}
R-M23-I-3
8/29/97
0818-1413
0.0400
0.0175
0.808
ND
ND
ND
{0.0900}
{0.0394}
{1.82}
{16.7}
{7.28}
{336}
Avenge of
1st and 2nd
Test run
{0.130}
{0.0902}
{3.53}
ND
ND
ND
{0.705}
{0.467}
{18.3}
{9.83}
{6.46}
{252}
() Not Detected. Value shown is the detection limit for that sample.
{} Estimated Maximum Possible Concentration.
-------
PCDD/PCDF Corrected Stack Gas Concentrations and 2378 TCDD Toxic Equivalent Concentrations
AynAtf ~Putntr « A" . Garner, North Carolina
US EPA Test Method 23 - PCDD/PCDF
Baghouse Inlet
RUN NUMBER
RUN DATE
RUN TIME
DIOXINS:
2378 TCDD
Total TCDD
12378 PeCDD
Total PeCDD
123478 HxCDD
1 23678 HxCDD
123789 HxCDD
Total HxCDD
1 234678 HpCDD
Total HpCDD
12346789 OCDD
Total PCDD
FURANS:
2378 TCDF
Total TCDF
12378 PeCDF
23478 PeCDF
Total PeCDF
123478 HxCDF
123678 HxCDF
234678 HxCDF
123789 HxCDF
Total HxCOF
1234678 HpCDF
1 234789 HpCDF
Total HpCDF
1 2346789 OCDF
Total PCDF
Total PCDD + PCDF
CONCENTRATION
(ng/dscmm, adjusted to 7% O2)
R-M23-I-1 R-M23-I-2 R-M23-I-3
08/27/97 08/28/97 08/29/97
0940-1227 0908-1428 0818-1413
ND NO ND
ND ND ND
ND ND ND
ND ND ND
ND ND ND
ND ND ND
ND ND ND
ND ND 0.0213
ND ND 0.149
{0.429} ND 0.363
11.9 10.1 17.3
{12.3} 10.1 17.7
ND ND ND
{0.221} 0.210 0.0107
ND ND ND
ND ND ND
0.576 0.408 {0.0107}
ND ND 0.021
ND ND ND
ND ND {0.00640}
ND ND ND
ND ND 0.0320
ND ND 0.0427
ND ND ND
ND {0.322} 0.0427
ND ND ND
{0.797} {0.940} {0.0960}
{13.1} {11.1} {178}
Average
of 1st & 2nd
Run
ND
ND
ND
ND
ND
ND
ND
ND
ND
{0.215}
11.0
{11.2}
ND
{0.215}
ND
ND
0.492
ND
ND
ND
ND
ND
ND
ND
{0.161}
ND
{0.868}
{12.1}
2378-TCDD
Toxic
Equivalent
Factor
1.000
0.500
0.100
0.100
0.100
0.010
0.001
0.100
0.050
0.500
0.100
0.100
0.100
0.100
0.010
0.010
0.001
2378 TOXIC EQUIVALENCIES
(ng/dscmm, adjusted to 7% O2)
R-M23-I-1 R-M23-I-2 R-M23-I-3
8/27/97 8/28/97 8/29/97
0940-1227 0908-1428 0818-1413
ND ND ND
"
ND ND ND
ND ND ND
ND ND ND
ND ND ND
ND ND 0.001
0.0119 0.0101 0.0173
0.0119 0.0101 0.0188
ND ND ND
ND ND ND
ND ND ND
ND ND 0.00213
ND ND ND
ND ND {0.000640}
ND ND ND
ND ND 0.000427
ND ND ND
ND ND ND
ND ND {0.00320}
0.0119 0.0101 {0.0220}
Average
of 1st & 2nd
Run
ND
ND
ND
ND
ND
ND
0.0110
0.0110
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
0.0110
-------
Summary of Stack Gas Parameters and Test Results
US EPA EMC Asphalt Concrete Emissions Testing • ftsmdu VUt,
US EPA Test Method 29 - Multiple Metals
Baghouse Inlet
Page 1 of 4
y
AH
Pbar
vm
Tm
•static
Ts
V,c
CO2
02
IM2
Vp
Ap
e
Dn
An
Vm(std)cf
Vjn(std) cm
Qm
PS
Bws
VW5td
1-BWS
Md
Ms
vs
A
Qa
Qscfm
Qscmm
I
RUN NUMBER
RUN DATE
RUN TIME
MEASURED DATA
Meter Box Correction Factor
Avg Meter Orifice Pressure, in. H20
Barometric Pressure, inches Hg
Sample Volume, ft3
Average Meter Temperature, °F
Stack Static Pressure, inches H2O
Average Stack Temperature, °F
Condensate Collected, ml
Carbon Dioxide content, % by volume
Oxygen content, % by volume
Nitrogen content, % by volume
Pilot Tube Coefficient
Average Square Root Ap, (in. H2O)1/2
Sample Run Duration, minutes
Nozzle Diameter, inches
CALCULATED DATA
Nozzle Area, ft2
Standard Meter Volume, ft3
Standard Meter Volume, m3
Average Sampling Rate, dscfm
Stack Pressure, inches Hg
Moisture, % by volume
Standard Water Vapor Volume, ft3
Dry Mole Fraction
Molecular Weight (d.b.), Ib/lb-mole
Molecular Weight (w.b.), Ib/lb-mole
Stack Gas Velocity, ft/s
Stack Area, ft2
Stack Gas Volumetric flow, acfm
Stack Gas Volumetric flow, dscfm
Stack Gas Volumetric flow, dscmm
Isokinetic Sampling Ratio, %
R-M29-I-1
«/27/97
-1000—1200
1.016
1.24
29.80
52.232
101
-1.8
304
422.5
4.6
14.2
81.2
0.84
0.6972
87
0.256
0.000357
49.883
1.413
0.573
29.67
28.5
19.887
0.715
29.30
26.08
49.7
16.20
48,345
23,687
671
109.7
R-M29-I-2
8/28/97
1019-1427
1.016
OJ298
29.60
64.379
102
-1.8
309
485.0
5.2
13.1
81.7
0.84
0.6977
200
0.194
0.000205
60.783
1.721
0.304
29.47
27.3
22.829
0.727
29.36
26.26
49.9
16.20
48,535
23,865
676
100.5
itr "B"
R-M29-I-3
8/29/97
0819-1403
1.016
0.400
29.60
85.398
96
-1.8
289
403.9
4.0
15.2
80.8
0.84
0.7185
240
0.196
0.000210
81.522
2.308
0.340
29.47
18.9
19.012
0.811
29.25
27.12
49.9
16.20
48,550
27,325
774
96.1
Average of
1st and 2nd
Test Runs
1.016
0.771
29.700
58.306
101.622
-1.800
306.083
453.750
4.900
13.650
81.450
0.840
0.697
143.500
0.225
0.000281
55.333
1.567
0.439
29.57
27.9
21.358
0.721
29.33
26.17
49.8
16.20
48,440
23,776
673
105.1
-------
Summary of Stack Gas Parameters and Test Results
US EPA EMC Asphalt Concrete Emissions Testing • KsryQiT Pt*
-------
Summary of Stack Gas Parameters and Test Results
US EPA EMC Asphalt Concrete Emissions Testing - Aspn*a fa
US EPA Test Method 29 - Multiple Metals
Baghouse Inlet
pg
pg/dscm
pg/dscm at 7%
g/hr
pg
pg/dscm
pg/dscm at 7%
g/hr
pg
pg/dscm
pg/dscm at 7%
g/hr
pg
pg/dscm
pg/dscm at 7%
g/hr
pg
pg/dscm
pg/dscm at 7%
g/hr
pg
pg/dscm
pg/dscm at 7%
g/hr
RUN NUMBER
RUN DATE
RUN TIME
EMISSIONS DATA -Continued
Chromium
Target Catch, pg
Concentration, pg/dscm
Concentration, pg/dscm at 7% O2
Emission Rate, g/hr
Colbalt
Target Catch, pg
Concentration, pg/dscm
Concentration, pg/dscm at 7% O2
Emission Rate, g/hr
Copper
Target Catch, pg
Concentration, pg/dscm
Concentration, pg/dscm at 7% O2
Emission Rate, g/hr
Lead
Target Catch, pg
Concentration, pg/dscm
Concentration, pg/dscm at 7% O2
Emission Rate, g/hr
Manganese
Target Catch, pg
Concentration, pg/dscm
Concentration, pg/dscm at 7% O2
Emission Rate, g/hr
Mercury
Target Catch, pg
Concentration, pg/dscm
Concentration, pg/dscm at 7% O2
Emission Rate, g/hr
Page 3 of 4
R-M29-I-1
8/27/97
-1000-1200
95.8
67.8
141
2.73
63.2
44.7
92.8
1.80
613
434
900
17.5
85.3
60.4
125
2.43
2,471
1,750
3,630
70.4
ND
ND
ND
ND
R-M29-I-2
8/28/97
1019-1427
88.3
"51.3
91.4
2.08
55.1
32.0
57.0
1.30
660
384
684
15.6
83.1
48.3
86.0
1.96
2,336
1,357
2,418
55.0
ND
ND
ND
ND
4<«r "g"
R-M29-I-3
8/29/97
0819-1403
76.8
33.3
81.2
1.55
45.5
19.7
48.1
0.915
607
263
641
12.2
82.7
35.8
87.4
1.66
2,251
975
2,377
45.3
ND
ND
ND
ND
Average of
1st and 2nd
Test Runs
92.1
59.6
116
2.41
59.2
38.4
74.9
1.55
636
409
792
16.5
84.2
54.3
106
2.19
2,404
1,553
3,024
62.7
ND
ND
ND
ND
-------
Summary of Stack Gas Parameters and Test Results
US EPA EMC Asphalt Concrete Emissions Testing • f,s,?miLr v-v .4*-; "3"
US EPA Test Method 29 - Multiple Metals
Baghouse Inlet
pg
pg/dscm
pg/dscm at 7%
g/hr
H9
pg/dscm
pg/dscm at 7%
g/hr
MS
pg/dscm
pg/dscm at 7%
g/hr
P9
pg/dscm
pg/dscm at 7%
g/hr
P9
pg/dscm
pg/dscm at 7%
g/hr
M9
pg/dscm
pg/dscm at 7%
g/hr
fl(W NUMBER
RUN DATE
RUN TIME
EMISSIONS DATA - Continued
Nickel
Target Catch, pg
Concentration, pg/dscm
Concentration, pg/dscm at 7% O2
Emission Rate, g/hr
Phosphorus
Target Catch, pg
Concentration, pg/dscm
Concentration, pg/dscm at 7% O2
Emission Rate, g/hr
Silver
Target Catch, pg
Concentration, pg/dscm
Concentration, pg/dscm at 7% O2
Emission Rate, g/hr
Selenium
Target Catch, pg
Concentration, pg/dscm
Concentration, pg/dscm at 7% O2
Emission Rate, g/hr
Thallium
Target Catch, pg
Concentration, pg/dscm
Concentration, pg/dscm at 7% O2
Emission Rate, g/hr
Zinc
Target Catch, pg
Concentration, pg/dscm
Concentration, pg/dscm at 7% O2
Emission Rate, g/hr
Page 4 of 4
R-M29-I-1
8/27/97
-1000-1200
59.0
4^.7
86.6
1.68
4,250
3,009
6,242
121
1.20
0.850
1.76
0.0342
ND
ND
ND
ND
12.2
8.64
17.9
0.348
761
539
1,118
21.7
R-M29-I-2
8/28/97
1019-1427
58.4
33.9
60.5
1.38
3,874
2,251
4,011
91.3
1.00
0.581
1.04
0.0236
0.396
0.230
0.410
0.00933
8.58
4.98
8.88
0.202
683
397
707
16.1
R-M29-I-3
8/29/97
0819-1403
50.3
21.8
53.1
1.01
5,010
2,170
5,292
101
0.671
0.291
0.709
0.0135
ND
ND
ND
ND
2.08
0.901
2.20
0.0418
553
239
584
11.1
Average o
1st and 2,
Test Rom
5
3
7.'
1
4,0'
2,6:
5,1:
1t
1.1
0,71
1.4
0.026
0,19
0.11
0.20.
0.0046!
10.3S
6.81
13.4C
Q27£
722
468
913
18.9
-------
-------
Appendix D.2
Computer Summaries
Baghouse Outlet - Method 9, 23 & 29
-------
-------
Date:
Start Time:
Stop Time:
8/29/97
0923
1023
Baghouse Outlet
Run Number: O-M9-3B
Net Run
Time,
minutes
0.25
0.50
0.75
1.00
1.25
1.50
1.75
2.00
2.25
2.50
2.75
3.00
3.25
3.50
3.75
4.00
4.25
4.50
4.75
5.00
5.25
5.50
5.75
6.00
6.25
6.50
6.75
7.00
7.25
7.50
7.75
8.00
8.25
8.50
8.75
9.00
9.25
9.50
9.75
10.00
10.25
10.50
10.75
11.00
11.25
11.50
11.75
12.00
HIGT
six-minute
rolling averages
percent opacity,
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
1.25
1.46
.46
.46
.25
.04
.25
.25
.25
.25
.25
.25
.25
.25
1.25
1.25
1.25
1.04
1.25
1.25
1.25
1.67
1.67
1.67
1.46
Net Run
Time,
minutes
12.25
12.50
12.75
13.00
13.25
13.50
13.75
14.00
14.25
14.50
14.75
15.00
15.25
15.50
15.75
16.00
16.25
16.50
16.75
17.00
17.25
17.50
17.75
18.00
18.25
18.50
18.75
19.00
19.25
19.50
19.75
20.00
20.25
20.50
20.75
21.00
21.25
21.50
21.75
22.00
22.25
22.50
22.75
23.00
23.25
23.50
23.75
24.00
six-minute
rolling averages
percent opacity,
.46
.46
.46
.67
.67
.46
.46
.67
.46
.46
.46
.46
.67
.67
.88
2.08
2.08
1.88
1.88
1.88
1.46
1.46
1.46
1.46
1.30
1.30
1.30
1.09
1.09
1.09
1.09
1.30
1.30
1.52
1.74
1.74
1.52
1.96
1.52
1.30
1.30
1.30
1.30
1.30
1.30
1.30
1.36
1.36
Net Run
Time,
minutes
24.25
24.50
24.75
25.00
25.25
25.50
25.75
26.00
26.25
26.50
26.75
27.00
27.25
27.50
27.75
28.00
28.25
28.50
28.75
29.00
29.25
29.50
29.75
30.00
30.25
30.50
30.75
31.00
31.25
31.50
31.75
32.00
32.25
32.50
32.75
33.00
33.25
33.50
33.75
34.00
34.25
34.50
34.75
35.00
35.25
35.50
35.75
36.00
six-minute
rolling averages
percent opacity,
1.30
1.30
.52
.52
.52
.52
.96
.52
.52
.30
.09
.09
.09
0.65
0.65
0.65
0.68
0.68
0.68
0.68
0.68
0.68
0.65
0.65
0.65
0.65
0.43
0.43
0.43
0.43
0.00
0.00
0.22
0.22
0.22
0.22
0.22
0.22
0.22
0.22
0.63
0.63
0.63
0.63
0.83
0.83
0.83
1.04
[ESt SlX-MINUTE BLOCK AVERAGE - 1.46 AVE
Net Run
Time,
minutes
36.25
36.50
36.75
37.00
37.25
37.50
37.75
38.00
38.25
38.50
38.75
39.00
39.25
39.50
39.75
40.00
40.25
40.50
40.75
41.00
41.25
41.50
41.75
42.00
42.25
42.50
42.75
43.00
43.25
43.50
43.75
44.00
44.25
44.50
44.75
45.00
45.25
45.50
45.75
46.00
46.25
46.50
46.75
47.00
47.25
47.50
47.75
48.00
RAGEO
six-minute
rolling averages
percent opacity,
1.04
.04
.04
.04
.25
.25
.25
.46
.25
.25
•25
.25
.25
.25
.25
.25
0.83
0.83
1.04
1.25
1.04
1.04
1.04
0.83
0.83
0.83
1.04
1.04
0.83
0.83
0.83
0.63
0.63
0.63
0.63
0.63
0.63
0.63
0.83
0.83
0.83
0.83
0.63
0.42
0.42
0.42
0.42
0.42
Net Run
Time,
minutes
48.25
48.50
48.75
49.00
49.25
49.50
49.75
50.00
50.25
50.50
50.75
51.00
51.25
51.50
51.75
52.00
52.25
52.50
52.75
53.00
53.25
53.50
53.75
54.00
54.25
54.50
54.75
55.00
55.25
55.50
55.75
56.00
56.25
56.50
56.75
57.00
57.25
57.50
57.75
58.00
58.25
58.50
58.75
59.00
59.25
59.50
59.75
60.00
six-minute
rolling averages
percent opacity,
0.42
0.42
0.21
0.21
0.21
0.21
0.22
0.23
0.23
0.23
0.23
0.23
0.23
0.45
0.23
0.23
0.45
0.45
0.45
0.45
0.45
0.68
0.91
0.91
1.36
1.36
1.36
1.36
1.36
1.36
1.30
1.25
1.25
1.25
NA*
NA*
NA*
NA*
NA*
NA*
NA*
NA*
NA*
NA*
NA*
NA*
NA*
NA*
r»AUTY DURING RUN = o.98
HIGHEST SIX-MINUTE ROLLING AVERAGE = 2.08
* Due to fugitive emission obstructions, a number of readings could not be made. Running averages included the time
lapses so that the net run time was shortened. NA indicates that for the time period, an average is Not Applicable.
-------
Date:
Start Time:
Stop Time:
8/29/97
1033
1133
Baghouse Outlet
Run Number: O-M9-3C
Net Run
Time,
minutes
0.2S
0.50
0.75
1.00
1.25
1.50
1.75
2.00
2.25
2.50
2.75
3.00
3.25
3.50
3.75
4.00
4.25
4.50
4.75
5.00
5.25
5.50
575
6.00
6.25
6.50
6.75
7.00
7.25
7.50
7.75
8.00
8.25
8.50
8.75
9.00
9.25
9.50
9.75
10.00
10.25
10.50
10.75
11.00
11.25
11.50
11.75
12.00
six-minute
rolling averages
percent opacity,
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
0.63
0.42
0.42
0.63
0.63
0.63
0.63
0.83
1.04
1.25
1.04
1.25
1.25
1.46
1.46
1.46
1.46
1.46
1.67
1.67
1.67
1.67
1.88
1.74
1.82
Net Run
Time,
minutes
12.25
12.50
12.75
13.00
13.25
13.50
13.75
14.00
14.25
14.50
14.75
15.00
15.25
15.50
15.75
16.00
16.25
16.50
16.75
17.00
17.25
17.50
17.75
18.00
18.25
18.50
1875
19.00
19.25
19.50
19.75
20.00
20.25
20.50
20.75
21.00
21.25
21.50
21.75
22.00
22.25
22.50
22.75
23.00
23.25
23.50
23.75
24.00
six-minute
rolling averages
percent opacity,
.82
.82
.59
.59
.59
.59
.36
.14
0.91
0.91
0.68
0.68
0.68
0.68
1.14
1.14
1.14
0.91
0.91
0.95
1.00
0.75
0.95
0.91
0.91
0.91
0.91
0.91
0.91
1.36
1.36
1.36
1.36
1.59
1.59
1.59
1.36
1.36
0.91
0.91
0.91
0.91
0.91
0.87
0.83
0.87
0.65
0.65
Net Run
Time,
minutes
24.25
24.50
24.75
25.00
25.25
25.50
25.75
26.00
26.25
26.50
26.75
27.00
27.25
27.50
27.75
28.00
28.25
28.50
28.75
29.00
29.25
29.50
29.75
30.00
30.25
30.50
30:75
31.00
31.25
31.50
31.75
32.00
32.25
32.50
32.75
33.00
33.25
33.50
33.75
34.00
34.25
34.50
34.75
35.00
35.25
35.50
35.75
36.00
six-minute
rolling averages
percent opacity,
0.65
0.65
0.65
0.65
0.65
0.22
0.22
0.22
0.43
0.22
0.22
0.22
0.22
0.22
0.22
0.43
0.43
0.43
0.43
0.43
0.65
0.63
0.63
0.63
0.63
0.63
0.63
0.63
0.63
0.63
0.63
0.63
0.42
0.42
0.42
0.63
0.63
0.83
0.83
0.63
0.63
0.63
0.63
0.65
0.43
0.43
0.43
0.43
HIGHEST SIX-MINUTE BLOCK AVERAGE = 1 .82 AVE
Net Run
Time,
minutes
36.25
36.50
36.75
37.00
37.25
37.50
37.75
38.00
38.25
38.50
38.75
39.00
39.25
39.50
39.75
40.00
40.25
40.50
40.75
41.00
41.25
41.50
41.75
42.00
42.25
42.50
42.75
43.00
43.25
43.50
43.75
44.00
44.25
44.50
44.75
45.00
45.25
45.50
45.75
46.00
46.25
46.50
46.75
47.00
47.25
47.50
47.75
48.00
six-minute
rolling averages
percent opacity,
0.43
0.43
0.43
0.43
0.43
0.43
0.43
0.43
0.43
0.43
0.43
0.22
0.22
0.22
0.22
0.22
0.22
0.65
0.65
0.63
0.63
0.63
0.63
0.63
0.63
0.83
0.83
0.83
0.83 '
0.83
0.83
0.83
0.83
0.83
0.83
0.83
0.83
0.63
0.63
0.63
0.83
0.42
0.42
0.42
0.43
0.43
0.43
0.43
Net Run
Time,
minutes
48.25
48.50
48.75
49.00
49.25
49.50
49.75
50.00
50.25
50.50
50.75
51.00
51.25
51.50
51.75
52.00
52.25
52.50
52.75
53.00
53.25
53.50
53.75
54.00
54.25
54.50
54.75
55.00
55.25
55.50
55.75
56.00
56.25
56.50
56.75
57.00
57.25
57.50
57.75
58.00
58.25
58.50
58.75
59.00
59.25
59.50
59.75
60.00
six-minute
rolling averages
percent opacity,
0.43
0.22
0.22
0.43
0.43
0.65
0.65
0.65
0.68
0.68
0.68
1.14
1.14
1.14
1.14
1.14
0.91
0.91
0.91
091
0.87
0.87
1.09
1.09
1.09
1.09
1.09
0.87
0.87
0.65
0.65
0.65
0.63
0.63
0.63
0.21
0.21
0.21
0.21
0.21
0.42
0.42
0.42
0.42
0.63
0.63
0.42
NA*
RAGE OPACITY DURING RUN = 0.75
HIGHEST SIX-MINUTE ROLLING AVERAGE = 1.88
* Due to fugitive emission obstructions, a number of readings
lapses so that the net run time was shortened. NA indicates
could not be made. Running averages included the time
that for the time period, an average is Not Applicable.
-------
Date: 8/29/97
Start Time: 1143
Stop Time: 1243
Baghouse Outlet
Run Number: O-M9-3D
Net Run
Time,
minutes
0.25
0.50
0.75
1.00
1.25
1.50
1.75
2.00
2.25
2.50
2.75
3.00
3.25
3.50
3.75
4.00
4.25
4.50
475
5.00
5.25
5.50
5.75
6.00
6.25
6.50
6.75
7.00
7.25
7.50
7.75
8.00
8.25
8.50
8.75
9.00
9.25
950
9.75
10.00
10.25
10.50
10.75
11.00
11.25
11.50
11.75
12.00
HIGI-
six-minute
rolling averages
percent opacity,
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
0.50
0.50
0.50
0.48
0.48
0.24
0.24
0.23
0.23
0.43
0.42
0.43
0.45
0.45
0.45
0.45
0.45
0.45
0.45
0.23
0.23
0.23
0.23
0.23
0.23
Net Run
Time,
minutes
12.25
12.50
12.75
13.00
13.25
13.50
13.75
14.00
14.25
14.50
14.75
15.00
15.25
15.50
15.75
16.00
16.25
16.50
16.75
17.00
17.25
17.50
17.75
18.00
1825
18.50
18.75
19.00
1925
19.50
19.75
20.00
20.25
20.50
20.75
21.00
21.25
21.50
21.75
22.00
22.25
22.50
22.75
23.00
23.25
23.50
23.75
24.00
six-minute
rolling averages
percent opacity,
0.23
0.23
0.23
0.23
0.23
0.23
0.23
0.23
0.00
0.00
0.00
0.00
0.00
0.00
0.00
0.00
0.21
0.21
0.42
0.42
0.42
0.42
0.42
0.42
0.63
0.63
0.63
0.63
0.63
0.65
0.65
0.65
0.87
0.91
0.91
0.91
0.91
0.91
0.95
1.43
1.43
1.43
.19
.19
.19
.19
.19
.19
Net Run
Time,
minutes
24.25
24.50
24.75
25.00
25.25
25.50
25.75
26.00
26.25
26.50
26.75
27.00
27.25
27.50
27.75
28.00
28.25
28.50
28.75
29.00
29.25
29.50
29.75
30.00
30.25
30.50
30.75
31.00
31.25
31.50
31.75
32.00
32.25
32.50
32.75
33.00
33.25
33.50
33.75
34.00
34.25
34.50
34.75
35.00
35.25
35.50
35.75
36.00
six-minute
rolling averages
percent opacity,
.19
.19
.19
.19
.19
.14
.14
1.14
0.91
0.87
0.87
0.87
0.87
0.87
0.83
0.42
0.21
0.21
0.21
0.21
0.21
0.22
0.22
0.22
0.00
0.00
0.00
0.00
0.45
0.68
0.68
0.68
0.68
0.68
0.68
0.68
1.14
1.14
1.14
1.14
1.14
1.14
1.14
1.14
1.14
1.09
1.09
1.09
IEST SIX-MINUTE BLOCK AVERAGE = 2.08 AVE
Net Run
Time,
minutes
36.25
36.50
36.75
37.00
37.25
37.50
37.75
38.00
38.25
38.50
38.75
39.00
39.25
39.50
39.75
40.00
40.25
40.50
40.75
41.00
41.25
41.50
41.75
42.00
42.25
42.50
42.75
43.00
43.25
43.50
43.75
44.00
44.25
44.50
44.75
45.00
45.25
45.50
45.75
46.00
46.25
46.50
46.75
47.00
47.25
47.50
47.75
48.00
RAGEO
six-minute
rolling averages
percent opacity,
1.09
1.09
1.30
1.30
0.91
0.71
0.71
0.75
0.79
0.79
' 0.79
0.79
0.28
0.28
0.56
0.56
0.56
0.56
1.11
l.ll
1.11
1.39
1.39
1.67
1.67
1.94
2.22
2.11
2.00
1.90
2.14
2.05
2.17
2.17
2.17
2.61
2.50
2.92
2.71
2.71
2.71
2.92
2.50
2.50
2.50
2.29
2.29
2.08
Net Run
Time,
minutes
48.25
48.50
48.75
49.00
49.25
49.50
49.75
50.00
50.25
50.50
50.75
51.00
51.25
51.50
51.75
52.00
52.25
52.50
52.75
53.00
53.25
53.50
53.75
54.00
54.25
54.50
54.75
55.00
55.25
55.50
55.75
56.00
56.25
56.50
56.75
57.00
57.25
57.50
57.75
58.00
58.25
58.50
58.75
59.00
59.25
59.50
59.75
60.00
^AcTl'Y DURING RUN =
six-minute
rolling averages
percent opacity,
2.29
2.08
.88
.88
.88
.88
.67
.67
.46
.88
.88
.46
.46
.04
.04
1.04
1.04
0.83
0.83
0.83
0.83
0.83
0.83
0.83
0.63
0.63
0.42
0.42
0.42
0.42
0.42
0.42
0.42
0.00
0.00
0.00
0.00
0.00
0.00
0.00
0.00
0.00
0.00
0.00
0.00
0.00
0.00
0.00
0.81
HIGHEST SIX-MINUTE ROLLING AVERAGE = 2.92
* Due to fugitive emission obstructions, a number of readings could not be made. Running averages included the time
lapses so that the net run time was shortened. NA indicates that for the time period, an average is Not Applicable.
-------
Summary of Stack Gas Parameters and Test Results
/hrrtHtr 7*ftorr"8" - Gary, North Carolina
US EPA Test Method 23 - PCDD / PCDF
Baghouse Outlet
Page 1 of 6
Y
AH
Pbar
vm
Tm
"static
Ts
Vlc
CO2
02
N2
CP
AP1"
0
Dn
An
Vm(std)
Vm(std)
PS
Bws
vwstd
1-BWS
Md
Ms
vs
A
Qa
Q,
Qs(cmm)
I
RUN NUMBER
RUN DATE
RUN TIME
MEASURED DATA
Meter Box Correction Factor
Avg Meter Orifice Pressure, in. H2O
Barometric Pressure, inches Hg
Sample Volume, ft3
Average Meter Temperature, °F
Stack Static Pressure, inches H20
Average Stack Temperature, °F
Condensate Collected, ml
Carbon Dioxide content, % by volume
Oxygen content, % by volume
Nitrogen content, % by volume
Pilot Tube Coefficient
Average Square Root Dp, (in. H2O)1/2
Sample Run Duration, minutes
Nozzle Diameter, inches
CALCULATED DATA
Nozzle Area, ft2
Standard Meter Volume, dscf
Standard Meter Volume, dscm
Stack Pressure, inches Hg
Moisture, % by volume
Standard Water Vapor Volume, ft3
Dry Mole Fraction
Molecular Weight (d.b.), Ib/lb-mole
Molecular Weight (w.b.), Ib/lb-mole
Stack Gas Velocity, ft/s
Stack Area, ft2
Stack Gas Volumetric flow, acfm
Stack Gas Volumetric flow, dscfm
Stack Gas Volumetric flow, dscmm
Isokinetic Sampling Ratio, %
R-M23-0-1
8/27/97
0940-1516
0.982
3.04
29.80
226.829
111
-1.5
283
2083.3
4.0
15.0
81.0
0.84
1 .0260
240
0.256
0.000357
206.781
5.855
29.69
32.2
98.061
0.678
29.24
25.62
72.8
11.23
49,075
23,450
664.0
115.5
R-M23-0-2
8/28/97
0746-1229
0.982
2.69
29.60
208.171
97
-1.4
287
1620.9
4.9
13.6
81.5
0.84
1.0561
240
0.256
0.000357
192.849
5.461
29.50
28.3
76.296
0.717
29.33
26.12
74.7
11.23
50,303
25,122
711.4
100.5
R-M23-O-3
8/29/97
0809-1236
0.982
2.86
29.60
226.098
98
-1.3
268
1087.4
3.0
16.3
80.7
0.84
1.0760
240
0.251
0.000344
209.298
5.927
29.50
19.6
51.184
0.804
29.13
26.94
74.0
11.23
49,832
28,612
810.2
99.6
Average of
1st and 2nd
Test Run
0.982
2.87
29.70
217.5
103.8
-1.45
285.0
1852.1
4.45
14.3
81.25
0.84
1.0410
240.0
0.256
0.000357
199.815
5.658
29.59
30.3
87.178
0.697
29.28
25.87
73.7
11.23
49,689
24,286
687.7
108.0
-------
Summary of Stack Gas Parameters and Test Results
fapwitrPiwrVp" - Gary, North Carolina
US EPA Test Method 23 - PCDD / PCDF
Baghouse Outlet
Page 2 of 6
(ng)
(ng/dscm)
(pg/hr)
(ng)
(ng/dscm)
(pg/hr)
(ng)
(ng/dscm)
(pg/hr)
(ng)
(ng/dscm)
(pg/hr)
(ng)
(ng/dscm)
(pg/hr)
(ng)
(ng/dscm)
(pg/hr)
RUN NUMBER
RUN DATE
RUN TIME
EMISSIONS DATA
DIOXINS:
2378 TCDD
Catch, ng
Concentration, ng/dscm, as measured
Emission Rate, pg/hr
Total TCDD
Catch, ng
Concentration, ng/dscm, as measured
Emission Rate, pg/hr
12378 PeCDD
Catch, ng
Concentration, ng/dscm, as measured
Emission Rate, pg/hr
Total PeCDD
Catch, ng
Concentration, ng/dscm, as measured
Emission Rate, pg/hr
123478 HxCDD
Catch, ng
Concentration, ng/dscm, as measured
Emission Rate, pg/hr
123678 HxCDD
Catch, ng
Concentration, ng/dscm, as measured
Emission Rate, pg/hr
R-M23-O-1
8/27/97
0940-1516
ND
ND
ND
ND
ND
ND
ND
ND
ND
{0.530}
{0.0905}
{3.61}
ND
ND
ND
ND
ND
ND
R-M23-0-2
8/28/97
0746-1229
ND -
ND
ND
ND
ND
ND
ND
ND
ND
{1.00}
{0.183}
{7.82}
ND
ND
ND
ND
ND
ND
R-M23-0-3
8/29/97
0809-1236
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
Average of
1st and 2nd
Test Run
ND
ND
ND
ND
ND
ND
ND
ND
ND
{0.765}
{0.137}
{5.71}
ND
ND
ND
ND
ND
ND
() Not Detected. Value shown is the detection limit for that sample.
{} Estimated Maximum Possible Concentration.
-------
Summary of Stack Gas Parameters and Test Results
/fspwfer ft/fc^'fc" - Gary, North Carolina
US EPA Test Method 23 - PCOD / PCDF
Baghouse Outlet
Page 3 of 6
(ng)
(ng/dscm)
(pg/hr)
(ng)
(ng/dscm)
(pg/hr)
(ng)
(ng/dscm)
(Mfl/hr)
(ng)
(ng/dscm)
(pg/hr)
(ng)
(ng/dscm)
(pg/hr)
(ng)
(ng/dscm)
(pg/hr)
RUN NUMBER
RUN DATE
RUN TIME
EMISSIONS DATA -Continued
DIOXINS - Continued
123789 HxCDD
Catch, ng
Concentration, ng/dscm, as measured
Emission Rate, pg/hr
Total HxCDD
Catch, ng
Concentration, ng/dscm, as measured
Emission Rate, pg/hr
1234678 HpCDD
Catch, ng
Concentration, ng/dscm, as measured
Emission Rate, pg/hr
Total HpCDD
Catch, ng
Concentration, ng/dscm, as measured
Emission Rate, pg/hr
1 2346789 OCDD
Catch, ng
Concentration, ng/dscm, as measured
Emission Rate, pg/hr
Total PCDD
Catch, ng
Concentration, ng/dscm, as measured
Emission Rate, pg/hr
R-M23-O-1
8/27/97
0940-1516
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
{0.530}
{0.0905}
{3.61}
R-M23-O-2
8/28/97
0746-1229
ND -
ND
ND
0.440
0.0806
3.44
ND
ND
ND
{1.00}
{0.183}
{7.82}
ND
ND
ND
{2.44}
{0.447}
{19.1}
R-M23-O-3
8/29/97
0809-1236
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
0.00
0.00
0.00
Average of
1st and 2nd
Test Run
ND
ND
ND
0.220
0.040
1.720
ND
ND
ND
{0.500}
{0.0916}
{3.91}
ND
ND
ND
{1.49}
{0.269}
{11-3}
() Not Detected. Value shown is the detection limit for that sample.
{} Estimated Maximum Possible Concentration.
-------
Summary of Stack Gas Parameters and Test Results
/krfMw-KjMT "8" - Gary, North Carolina
US EPA Test Method 23 - PCDD / PCDF
Baghouse Outlet
Page 4 of 6
(ng)
(ng/dscm)
(ug/hr)
(ng)
(ng/dscm)
(pg/hr)
(ng)
(ng/dscm)
(pg/hr)
(ng)
(ng/dscm)
(pg/hr)
(ng)
(ng/dscm)
(pg/hr)
(ng)
(ng/dscm)
(pg/hr)
RUN NUMBER
RUN DATE
RUN TIME
EMISSIONS DATA- Continued
FURANS
2378 TCDF
Catch, ng
Concentration, ng/dscm, as measured
Emission Rate, pg/hr
Total TCDF
Catch, ng
Concentration, ng/dscm, as measured
Emission Rate, pg/hr
12378 PeCDF
Catch, ng
Concentration, ng/dscm, as measured
Emission Rate, pg/hr
23478 PeCDF
Catch, ng
Concentration, ng/dscm, as measured
Emission Rate, pg/hr
Total PeCDF
Catch, ng
Concentration, ng/dscm, as measured
Emission Rate, pg/hr
1 23478 HxCDF
Catch, ng
Concentration, ng/dscm, as measured
Emission Rate, pg/hr
R-M23-O-1
8/27/97
0940-1516
ND
ND
ND
0.150
0.0256
1.02
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
R-M23-O-2
8/28/97
0746-1229
ND .
ND
ND
ND
ND
ND
{0.240}
{0.0439}
{1.88}
ND
ND
ND
{0.410}
{0.0751}
{3.20}
ND
ND
ND
R-M23-O-3
8/29/97
0809-1236
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
{0.0200}
{0.00337}
{0.164}
ND
ND
ND
1
Average of
1st and 2nd
Test Run
ND
ND
ND
0.075
0.013
0.510
{0.120}
{0.0220}
{0.938}
ND
ND
ND
{0.205}
{0.0375}
{1.60}
ND
ND
ND
() Not Detected. Value shown is the detection limit for that sample.
{} Estimated Maximum Possible Concentration.
-------
Summary of Stack Gas Parameters and Test Results
fkprtitcr Put** "8" - Gary, North Carolina
US EPA Test Method 23 - PCDD / PCDF
Baghouse Outlet
Page 5 of 6
(ng)
(ng/dscm)
(pg/hr)
(ng)
(ng/dscm)
(pg/hr)
(ng)
(ng/dscm)
(pg/hr)
(ng)
(ng/dscm)
(pg/hr)
(ng)
(ng/dscm)
(pg/hr)
(ng)
(ng/dscm)
(pg/hr)
RUN NUMBER
RUN DATE
RUN TIME
EMISSIONS DATA - Continued
Furans - Continued
1 23678 HxCDF
Catch, ng
Concentration, ng/dscm, as measured
Emission Rate, jjg/hr
234678 HxCDF
Catch, ng
Concentration, ng/dscm, as measured
Emission Rate, pg/hr
123789 HxCDF
Catch, ng
Concentration, ng/dscm, as measured
Emission Rate, pg/hr
Total HxCDF
Catch, ng
Concentration, ng/dscm, as measured
Emission Rate, pg/hr
1 234678 HpCDF
Catch, ng
Concentration, ng/dscm, as measured
Emission Rate, pg/hr
1234789 HpCDF
Catch, ng
Concentration, ng/dscm, as measured
Emission Rate, pg/hr
R-M23-O-1
8/27/97
0940-1516
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
R-M23-O-2
8/28/97
0746-1229
ND
ND
ND
ND
ND
ND
{0.240}
{0.0439}
{1.88}
{0.460}
{0.0842}
{3.60}
ND
ND
ND
ND
ND
ND
R-M23-O-3
8/29/97
0809-1236
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
Average of
1st and 2nd
Test Run
ND
ND
ND
ND
ND
ND
{0.120}
{0.0220}
{0.938}
{0.230}
{0.0421}
{1 .80}
ND
ND
ND
ND
ND
ND
() Not Detected. Value shown is the detection limit for that sample.
{} Estimated Maximum Possible Concentration.
-------
Summary of Stack Gas Parameters and Test Results
ftspttAir 7W-"g" - Gary, North Carolina
US EPA Test Method 23 - PCDD / PCDF
Baghouse Outlet
Page 6 of 6
(ng)
(ng/dscm)
(pg/hr)
(ng)
(ng/dscm)
(Mg/hr)
(ng)
(ng/dscm)
(pg/hr)
(ng)
(ng/dscm)
(|jg/hr)
RUN NUMBER
RUN DATE
RUN TIME
EMISSIONS DATA - Continued
Furans - Continued
Total HpCDF
Catch, ng
Concentration, ng/dscm, as measured
Emission Rate, pg/hr
1 2346789 OCDF
Catch, ng
Concentration, ng/dscm, as measured
Emission Rate, pg/hr
Total PCDF
Catch, ng
Concentration, ng/dscm, as measured
Emission Rate, pg/hr
Total PCDD + PCDF
Catch, ng
Concentration, ng/dscm, as measured
Emission Rate, pg/hr
R-M23-O-1
8/27/97
0940-1516
ND
ND
ND
ND
ND
ND
0.150
0.0256
1.02
{0.680}
{0.116}
{4.63}
R-M23-O-2
8/28/97
0746-1229
{0.360}
{0.0659}
{2.81}
ND
ND
ND
{1.23}
{0.225}
{9.61}
{3.67}
{0.672}
{28.7}
R-M23-O-3
8/29/97
0809-1236
ND
ND
ND
ND
ND
ND
{0.0200}
{0.00337}
{0.164}
{0.0200}
{0.00337}
{0.164}
Average of
1st and 2nd
Test Run
{0.180}
{0.0330}
{1.41}
ND
ND
ND
{0.690}
{0.125}
{5.32}
{2.18}
{0.394}
{16.7}
() Not Detected. Value shown is the detection limit for that sample.
{} Estimated Maximum Possible Concentration.
-------
PCDD/PCDF Corrected Stack Gas Concentrations and 2378 TCDD Toxic Equivalent Concentrations
ftsrtttii-r -PUM "8"- Gary, North Carolina
US EPA Test Method 23 - CDD/CDF
Baghouse Outlet
RUN NUMBER
RUN DATE
RUN TIME
DIOXINS:
2378 TCDD
Total TCDD
12378PeCDD
Total PeCDD
1 23478 HxCDD
123678 HxCDD
123789 HxCDD
Total HxCDD
1 234678 HpCDD
Total HpCDD
1 2346789 OCDD
Total PCDD
FURANS:
2378 TCDF
Total TCDF
12378 PeCDF
23478 PeCDF
Total PeCDF
123478 HxCDF
1 23678 HxCDF
234678 HxCDF
123789 HxCDF
Total HxCDF
1234678 HpCDF
1234789 HpCDF
Total HpCDF
12346789 OCDF
Total PCDF
Total PCDD+PCDF
CONCENTRATION
(ng/dscm, adjusted to 7% O2)
R-M23-O-1 R-M23-O-2 R-M23-O-3
08/27/97 08/28/97 08/29/97
0940-1516 0746-1229 0809-1236
ND ND ND
ND ND ND
ND ND ND
{0.213} {0.349} ND
ND ND ND
ND ND ND
ND ND ND
ND 0.153 ND
ND ND ND
ND {0.349} ND
ND ND ND
{0.213} {0.851} 0.00
ND ND ND
0.060 ND ND
ND {0.0837} ND
ND ND ND
ND {0.143} {0.0102}
ND ND ND
ND ND ND
ND ND ND
ND {0.0837} ND
ND {0.160} ND
ND ND ND
ND ND ND
ND {0 126} ND
ND ND ND
0.0604 {0.429} {0.0102}
{0.274} {1.28} {0.0102}
Average of
Island 2nd
Test Run
ND
ND
ND
{0.281}
ND
ND
ND
0.0767
ND
{0.174}
ND
{0.532}
ND
0.0302
{0.0418}
ND
{0.0715}
ND
ND
ND
{0.0418}
{0.0802}
ND
ND
{0.0628}
ND
{0.245}
{0.777}
2378-TCDD
Toxic
Equivalent
Factor
1.000
0.500
0.100
0.100
0.100
0.010
0001
0.100
0.050
0.500
0.100
0.100
0.100
0.100
0.010
0.010
0.001
2378 TOXIC EQUIVALENCIES
(ng/dscm, adjusted to 7% O2)
R-M23-O-1 R-M23-O-2 R-M23-O-3
8/27/97 8/28/97 8/29/97
0940-1516 0746-1229 0809-1236
ND ND ND
ND ND ND
ND ND ND
ND ND ND
ND ND ND
ND ND ND
ND ND ND
ND ND ND
ND ND ND
ND {0.00418} ND
ND ND ND
ND ND ND
ND ND ND
ND ND ND
ND {0.00837} ND
ND ND ND
ND ND ND
ND ND ND
ND {0.0126} ND
ND {0.0126} ND
Average of
1st and 2i
'est Run
ND
ND
ND
ND
ND
ND
ND
ND
ND
{0.0021
ND
ND
ND
ND
{0.004
ND
NC
NC
{O.OOf
{O.OOt
-------
Summary of Stack Gas Parameters and Test Results
US EPA EMC Asphalt Concrete Emissions Testing /fsprf/hr fcfatr "8 "
US EPA Test Method 29 - Multiple Metals
Baghouse Outlet
Page 1 of 4
Y
AH
Pbar
vm
Tm
Pstatic
Ts
V,c
CO2
02
N2
cp
Ap1/2
0
Dn
An
Vm(std) cf
* m(std) cm
Qm
PS
Bws
Vwstd
1-BWS
Md
Ms
Vs
A
Qa
Qscfm
Qscmm
I
RUN NUMBER
RUN DATE
RUN TIME
MEASURED DATA
Meter Box Correction Factor
Avg Meter Orifice Pressure, in. H2O
Barometric Pressure, inches Hg
Sample Volume, ft3
Average Meter Temperature, °F
Stack Static Pressure, inches H2O
Average Stack Temperature, °F
Condensate Collected, ml
Carbon Dioxide content, % by volume
Oxygen content, % by volume
Nitrogen content, % by volume
Pitot Tube Coefficient
Average Square Root Ap, (in. H2O)1/2
Sample Run Duration, minutes
Nozzle Diameter, inches
CALCULATED DATA
Nozzle Area, ft2
Standard Meter Volume, ft3
Standard Meter Volume, m3
Average Sampling Rate, dscfm
Stack Pressure, inches Hg
Moisture, % by volume
Standard Water Vapor Volume, ft3
Dry Mole Fraction
Molecular Weight (d.b.), Ib/lb-mole
Molecular Weight (w.b.), Ib/lb-mole
Stack Gas Velocity, ft/s
Stack Area, ft2
Stack Gas Volumetric flow, acfrn
Stack Gas Volumetric flow, dscfm
Stack Gas Volumetric flow, dscmm
tsokinetic Sampling Ratio, %
R-M29-O-1
8/27/97
0940-1516
0.965
2.96
29.80
237.264
109
-0.42
289
1632.0
4.0
15.0
81.0
0.84
1.0773
240
0.252
0.000346
213.024
6.032
0.888
29.77
26.5
76.818
0.735
29.24
26.26
75.7
11.23
51,035
26,285
744
109.5
R-M29-O-2
8/28/97
0746-1229
0.965
2.14
29.60'
200.329
97
-0.4
292
1484.6
4.9
13.6
81.5
0.84
1.0386
240
0.252
0.000346
182.236
5.160
0.759
29.57
27.7
69.880
0.723
29.33
26.19
73.5
11.23
49,516
24,833
703
99.2
R-M29-O-3
8/29/97
0809-1236
0.965
2.80
29.60
227.316
100
-0.42
274
1147.1
3.0
16.3
80.7
0.84
1.0852
240
0.252
0.000346
205.914
5.831
0.858
29.57
20.8
53.994
0.792
29.13
26.82
75.0
11.23
50,521
28,440
805
97.8
Average of
1st and 2nd
Test Runs
0.965
2.55
29.70
218.797
103
-0.41
291
1558.3
4.5
14.3
81.3
0.84
1.0580
240
0.252
0.000346
197.630
5.596
0.823
29.67
27.1
73.349
0.729
29.28
26.22
74.6
11.23
50,276
25,559
724
104.3
-------
Summary of Stack Gas Parametere and Test Results
US EPA EMC Asphalt Concrete Emissions Testing - AsTrMcr PL
*urwtf"
US EPA Test Method 29 - Multiple Metals
RUN NUMBER
RUN DATE
RUN TIME
EMISSIONS DATA
Particulate Matter
g Target Catch, g
gr/dscf Concentration, gr/dscf
gr/dscf at 7% Concentration, gr/dscf at 7% O2
g/dscm Concentration, g/dscm
g/dscm at 7% Concentration, g/dscm at 7% O2
Ib/hr Emission Rate, Ib/hr
kg/hr Emission Rate, kg/hr
Antimony
pg Target Catch, pg
pg/dscm Concentration, pg/dscm
pg/dscm at 7% Concentration, pg/dscm at 7% O2
g/hr Emission Rate, g/hr
Arsenic
pg Target Catch, pg
pg/dscm Concentration, pg/dscm
pg/dscm at 7% Concentration, pg/dscm at 7% O2
g/hr Emission Rate, g/hr
Barium
pg Target Catch, pg
pg/dscm Concentration, pg/dscm
pg/dscm at 7% Concentration, pg/dscm at 7% O2
g/hr Emission Rate, g/hr
Beryllium
pg Target Catch, pg
pg/dscm Concentration, pg/dscm
pg/dscm at 7% Concentration, pg/dscm at 7% O2
g/hr Emission Rate, g/hr
Cadmium
pg Target Catch, pg
pg/dscm Concentration, pg/dscm
pg/dscm at 7% Concentration, pg/dscm at 7% O2
g/hr Emission Rate, g/hr
Baghouse Outlet
Page 2 of 4
R-M29-O-1
8/27/97
0940-1516
0.1148
0.00832
0.0196
0.0190
0.0448
1.87
0.850
3.84
0.637
1.50
0.0284
ND
ND
ND
ND
54.9
9.10
21.4
0.406
ND
ND
ND
ND
0.479
0.0794
0.187
0.00355
R-M29-0-2
8/28/97
0746-1229
0.0982
0.00832
0.01 58
0.0190
0.0362
1.77
0.803
3.58
0.693
1.32
0.0292
ND
ND
ND
ND
40.9
7.92
15.1
0.334
ND
ND
ND
ND
0.366
0.0708
0.135
0.00299
R-M29-0-3 Average of
8/29/97 1st and 2nd
0809-1236 Test
0.1766
0.01324
0.0400
0.0303
0.0915
3.23
1.463
3.91
0.671
2.03
0.0324
ND
ND
ND
ND
69.9
12.0
36.2
0.579
ND
ND
ND
ND
0.196
0.0336
0.102
0.00162
Runs
0.1065
0.0083
0.0177
0.0190
0.0405
1.82
0.8264
3.71
0.665
1.41
0.0288
ND
ND
ND
ND
47.9
8.51
18.3
0.370
ND
ND
ND
ND
0.422
0.0751
0.161
0.00327
-------
Summary of Stack Gas Parameters and Test Results
US EPA EMC Asphalt Concrete Emissions Testing • /Jsp/Mtr Tutor " £ "
US EPA Test Method 29 - Multiple Metals
Baghouse Outlet
Page 3 of 4
pg
pg/dscm
pg/dscm at 7%
g/hr
M9
pg/dscm
Mg/dscm at 7%
g/hr
P9
pg/dscm
pg/dscm at 7%
g/hr
M9
pg/dscm
pg/dscm at 7%
g/hr
Mg
pg/dscm
pg/dscm at 7%
g/hr
pg
pg/dscm
pg/dscm at 7%
g/hr
RUN NUMBER
RUN DATE
RUN TIME
EMISSIONS DATA - Continued
Chromium
Target Catch, pg
Concentration, pg/dscm
Concentration, pg/dscm at 7% 02
Emission Rate, g/hr
Colbalt
Target Catch, pg
Concentration, pg/dscm
Concentration, pg/dscm at 7% O2
Emission Rate, g/hr
Copper
Target Catch, pg
Concentration, pg/dscm
Concentration, pg/dscm at 7% O2
Emission Rate, g/hr
Lead
Target Catch, pg
Concentration, pg/dscm
Concentration, pg/dscm at 7% O2
Emission Rate, g/hr
Manganese
Target Catch, pg
Concentration, pg/dscm
Concentration, pg/dscm at 7% O2
Emission Rate, g/hr
Mercury
Target Catch, pg
Concentration, pg/dscm
Concentration, pg/dscm at 7% O2
Emission Rate, g/hr
R-M29-O-1
«/27/97
0940-1516
13.2
2.19
5.16
0.0978
ND
ND
ND
ND
9.29
1.54
3.63
0.0688
8.54
1.42
3.34
0.0632
70.0
11.6
27.4
0.519
ND
ND
ND
ND
R-M29-O-2
8/28/97
0746-1229
11.0
2.14
4.0J
0.0901
ND
ND
ND
ND
7.14
1.38
2.63
0.0584
5.30
1.03
1.95
0.0433
74.8
14.5
27.6
0.612
ND
ND
ND
ND
R-M29-O-3
8/29/97
0809-1236
12.6
2.16
6.53
0.104
ND
ND
ND
ND
15.0
2.57
7.77
0.124
6.09
1.04
3.16
0.0505
116.3
19.9
60.3
0.964
ND
ND
ND
ND
Average of
1st and 2nd
Test Runs
12.1
2.16
4.61
0.0939
ND
ND
ND
ND
8.2
1.46
3.13
0.0636
6.92
1.22
2.64
0.0533
72.4
13.1
27.5
0.565
ND
ND
ND
ND
-------
Summary of Stack Gas Parameters and Test Results
US EPA EMC Asphalt Concrete Emissions Testing • '4$l&Atf~ J*^*r
US EPA Test Method 29 • Multiple Metals
Baghouse Outlet
Page 4 of 4
pg
pg/dscm
pg/dscm at 7%
g/hr
pg
pg/dscm
pg/dscm at 7%
g/hr
pg
pg/dscm
pg/dscm at 7%
g/hr
pg
pg/dscm
pg/dscm at 7%
g/hr
pg
pg/dscm
pg/dscm at 7%
g/hr
pg
pg/dscm
pg/dscm at 7%
g/hr
RUN NUMBER
RUN DATE
RUN TIME
EMISSIONS DATA - Continued
Nickel
Target Catch, pg
Concentration, pg/dscm
Concentration, pg/dscm at 7% O2
Emission Rate, g/hr
Phosphorus
Target Catch, pg
Concentration, pg/dscm
Concentration, pg/dscm at 7% O2
Emission Rate, g/hr
Silver
Target Catch, pg
Concentration, pg/dscm
Concentration, pg/dscm at 7% O2
Emission Rate, g/hr
Selenium
Target Catch, pg
Concentration, pg/dscm
Concentration, pg/dscm at 7% O2
Emission Rate, g/hr
Thallium
Target Catch, pg
Concentration, pg/dscm
Concentration, pg/dscm at 7% O2
Emission Rate, g/hr
Zinc
Target Catch, pg
Concentration, pg/dscm
Concentration, pg/dscm at 7% O2
Emission Rate, g/hr
r "g"
R-M29-O-1 R-M29-O-2 R-M29-O-3 Avenge of
a/27/97 8/28/97 8/29/97 1st and 2nd
0940-1516 0746-1229 0809-1236 Test Runs
9.37
1.55
3.66
0.0694
110
18.2
42.9
0.814
0.378
0.0627
0.148
0.00280
5.63
0.934
2.20
0.0417
ND
ND
ND
ND
44.3
7.34
17.3
0.328
6.50
1.26
2.43
0.0531
115
22.2
42.3
0.937
0.217
0.0421
0.080
0.00177
4.58
0.888
1.69
0.0375
ND
ND
ND
ND
25.9
5.01
9.54
0.211
8.13
1.39
4.21
0.0674
145
24.9
75.2
1.20
ND
ND
ND
ND
4.91
0.843
2.55
0.0407
ND
ND
ND
ND
32.8
5.63
17.0
0.272
7.93
1.41
3.03
0.0612
112
20.2
42.6
0.876
0.298
0.0524
0.114
0.00229
2.29
0.911
1.95
0.0396
ND
ND
ND
ND
35.1
6.18
13.4
0.270
-------
APPENDIX E
QA/QC DATA AND CERTIFICATIONS
-------
-------
\
TEMPERATURE SENSOR CALIBRATION FORM
Temperature Sensor No.
Ambient Temp. °F 37
-4
Reference Temp. Sensor:
Sensor Tvne V. - "\ Ic Length 6"-
Barometric Pressure, "Hg 7Q.*K
Date
lv/7«fc*
io|?< k>
loMto
Ref.
Point
No.
1
2
3
1
2
3
1
2
3
1
2
3
1
2
3
1
2
3
Temp.
Source
1C* UxJLr
ftJ». Gvr
to vJU.
Temp. °F
Ref.
Sensor
(V*)-?>-l
(&i) ^
^ 7 10
Test
Sensor
CW 36
c<^) ^r
((rffi^ Zc^
Temp.
Diff. %
C.20
-O.^p
o.\r .
Within
Limits
Y/N
. V
V
V
Calibrated
By
Ml*
VhOfl\
VAOVK
*
*
Temp. Diff
(Jtef ' Temp + 40) " ( Test
460)
,
(Ref. Temp. + 460)
x 100 S 1 5 \
-------
TEMPERATURE SENSOR CALIBRATION FORM
Temperature Sensor No. fe-T-U
Ambient Temp. °F
Reference Temp. Sensor:
Sensor Type fc "\ Ic Length 6
Barometric Pressure, "Hg V{ .c»6
Date
iota ta
lo/?^
Ic.^(=t1-
Ref.
Point
No.
1
2
3
1
2
3
1
2
3
1
2
3
1
2
3
1
2
3
Temp.
Source
tf Uc-W
a«J»- &«.''
Vxxl-s «J*
Temp. °F
Ref.
Sensor
3u
•^•2-
?u
Test
Sensor
3?
^
7(0
•
Temp.
Diff. %
Whhin
Limits
Y/N
Calibrated
By
% Temp. Diff
*
(gaf '
. Temp. + 460)
10°
-------
V
TEMPERATURE SENSOR CALIBRATION FORM
Temperature Sensor No.
Ambient Temp. °F
Reference Temp. Sensor:
tew
Sensor Type JL_3l£— Length 4j
_ Barometric Pressure, "Hg ~~ ' ~
Date
re i\ M"»
i(h»fa
1<^?<|<1*
Ref.
Point
No.
1
2
3
1
2
3
1
2
3
1
2
3
1
2
3
1
2
3
Temp.
Source
a* uir
Ci J». 4t*y
P. (JtJU--
Temp. °F
Ref.
Sensor
4*) T2-
(£^74
b^ 7^
Test
Sensor
4^s) S3
53t)^Z
^ 2/1
Temp.
Diff . %
- G.Z-o
0.3T-
o.\^
Within
Limits
Y/N
V
y
Y
Calibrated
By
BY^f*
^^
^>«n
, Temp. «„
-( rest
46o,
(Ref. Temp. + 460)
„ 100 s 1-5
-------
TEMPERATURE SENSOR CALIBRATION FORM
Temperature Sensor No.
Ambient Temp. °F
30.
Sensor Type
Length
4-1
Barometric Pressure, "Hg 33-
Reference Temp. Sensor:
Date
^he^n-
<* leffr
Ref.
Point
No.
1
2
s|l«H 3
1
2
3
1
2
3
1
2
3
1
2
3
1
2
3
Temp.
Source
«*\J*i
P V«*<^
>-Uit-W.
Temp. °F
Ref.
Sensor
4i
^%
240
Test
Sensor
4-1
^
\z-
Temp.
Diff. %
6
0
-. 0,3o
Within
Limits
Y/N
Y
V
V
Calibrated
By
t*W\
CMi*
*Vv»JvW
* Temn Diff - (Rsf' TemP * 4!0) " ( TG3t TfP' * 460) x 100
* TemP- Dirr (Ref. Temo. + 460)
-------
Probe or Pitot No.
Pilot Tube Inspection
I.EV5I.
*-—X
o
BULLSEYS LEVEL -
-pi
8
U"
Thermocouple Calibration
Type of Reference Thermometer
Barometric Pressure -, *
_.inHg
Date
Tube Assembly Level?
Ports Damaged?
-10°•
,^10
~,0/7
,00^
.vt
,r
,"3^r
.^^.Ob^
.*•/<)?_< $5*573
Date
Ambient Temperature_
Source
A.fc.v.f
_ Tc<. t,«
/f»f- u/,.^
Reference
Temperature
^
2£
f7^
Thermocouple
Temperature
n
%i
r^6
Absolute Temperature
Difference1
-.011
-M(*
0
Temp., "F » 460) - (ThermocoupUT&mp., "F - 460)
fD/,/" T • IT /trns
-------
Probe or Pitot No.
G
Pitot Tube Inspection
0
i— i ^
1 BULISEYE LEVEL)— <^
1 ^
rral IV ? )l
B«, l^M
,_n-,.JU
i.i
~z^"pi iGli
. ~ir^v __p 7 L^s^
• -• - -^.\
~^|k^
•^ 4Q '"
1 \feJs^X
\-- — ^ '
Thermocouple Calibration
Type of Reference Thermometer ^ ^tvj :« 0 /««
Date
Tube Assembly Level?
Ports Damaged?
-10-<«1<+10- ..
-10°°
o¥
l.fl/3
• ,^v
^>
,5T
•J-/
,?70
jjt+ d^"^ s&
vQ/ — $j^*~^¥f>
Date Z/H/f ?
Barometric Pressure ^^^^ ^^S ' Ambient Temperature f-07 °F
Source • Reference
Temperature
tyt ^.^ Uf
>Lvir f /c/2
1 (Ref. Temp., 'F * 460) - (1
Thermocouple Absolute Temperature
Temperature Difference1
H 1 ~. <)<;^
/O/ f<502
^^ 0
'hermocovpleTemp., "F • 460)
(Ref T.mn
-------
• m •
Inspection Data Sheet
Company Hame:
«• MHn •«!•«• OT»M> KM m f« wwr IM I
MU « KM MM M MM M •!&* tint IMM. j
Pre-sample
Date
Post Sample
Date fO-f3-1"7
level?
obstructions?
damaged?
-10° < 01 < +10*
-10* < a» < -HO0
-5" < Bi < -H5°
-5° < 82 < +5°
Y
6
A
•?nC .5-03
1.05 Dt < Pa < 1.5 Dt
. .
1.05 Dt < PD < 1.5 Ot
3/16" '< Dt * 3/8
A tan Y < 0.125"
A tan 9 < 0.03125"
Pa • Pb ± 0.063"
OOS1H.
Comments:
P1tot tube/probe number
meets or exceeds all specifications
criteria and/or applicable design features* and is hereby assigned a
pi tot tube calibration factor of 0.84.
•
Signature
*• Date
•SM 40 CfA 60. vol. *Z. No. 1*0. Mttfio* 2. »tHfy tlM nlniBUB
2 l«e» tttMck of tiw tntn«ocouplt MM tin «tm«« 3/4 incft
MMritton oitMtii tin pltot tuM «•« tM noszlt «i >MM «t
tat top of tnis M««.
-------
Date OS-Aug-87 Meter Box Number M5-4
Calibrated By B Palm Initials t?0 .
NumberofRuns 5 ^YcJ»V».
Meter Y 1.016
Vw.Wt
Vw.fin
Vw, total
Pb
tw
Tw+460
BRY f5A^
Previous Y 1.024
Vm. init
Vm.fln
Vm. total
Tdii
Td«
Tdol
Tdof
Td.avg
Td+460
Time, mln
Time, sec
Time Total
dH
PALIBRATIC
Y
dH©
Y tolerance from avg *
dH® tol. from avg •*
AVERAGE Y
AVERAGE dH®
RUN1
907.127
912.513
5.386
29.80
64
544
MFTPR
653.019
658.402
5.383
65
69
82
84
85
545
13
30
13.50
0.50
IN RESULTS
1.017
1.764
0.00
0.05
1.021
1.818
RUN 2
912.675
918.262
5.387
29.80
84
544
658.758
664.147
5.389
86
93
84
86
87.75
547.75
9
30
9.50
1.00
1.020
1.740
0.00
0.08
RUNS
918.094
924.06
5.366
29.60
84
544
664.577
669.948
5.371
89
97
86
87
89.75
549.75
8
0
8.00
1.50
1.022
1.861
-0.00
-0.04
RUN 4
924.597
929.999
5.402
29.80
84
544
670.486
675.901
5.415
92
100
88
88
92
552
7
0
7.00
2.00
1.023
1.869
-0.00
-0.05
RUNS
930.307
936.958
6.651
29.80
65
545
676.205
682.864
6.659
93
104
88
89
93.5
553.5
7
0
7.00
3.00
1.023
1.854
•0.00
•0.04
RUN 6
0
0
0
29.80
0
460
0
0
0
0
0
0
0
0
460
0
0
0.00
4.00
0.000
0.000
1.02
1.82
Y error (vs prior Y) ***
-0.3%
* must be no greater than +/- 0.02
** must be no greater than +/- 0.20
*•• must be no greater than +/- 5%
-------
Calibrated By Richard Initial* a L)ft/\
Number of Runs 3 Jw^'v I) *
_._...__ RFFFBFNPF TF3T MFTFR ........
Meter Y 1.016
Vw, Wt
Vw.fin
Vw, total
Pb
tw
Tw+460
RUN1
643.779
652.1
8.321
29.87
61
521
RUN 2
652.614
662.322
9.708
29.87
62
522
RUNS
662.945
670.381
7.436
29.87
62
522
RUN 4
0
0
0
29.87
0
460
RUNS
0
0
0
29.87
0
460
. , nnv f\ A
-------
Date OS-Aug-97
Calibrated By B Palm
Number of Run* 5
Mater Box Number M5-9
REFERENCE TEST METER
Mater Y 1.016
Vw.tntt
Vw.fin
Vw, total
Pb
RUN1
873.304
878.349
5.045
29.80
tw 79.5
Tw+460 539.5
RUN 2
878.537
883.6
5.083
29.80
80.5
540.5
RUNS
883.95
89O.707
6.757
29.80
81
541
RUN 4
891.057
897.317
6.26
29.80
81.5
541.5
RUNS
899.221
905.513
6.292
29.80
82
542
RUN 6
0
0
0
29.80
0
480
Previous Y 0.996
Vm, Wt
Vm.fln
Vm. total
TdH
Td»
Tdol
Tdof
Td.avg
Td+460
Time, mln
Time, sac
Time Total
dH
pAI IPtO Al
Y
dH©
Y tolerence from avg *
dH@ toL from avg **
AVERAGE Y
AVERAGE dH®
717.968
723.025
5.057
79
84
78
80
80.25
540.25
12
30
12.50
O.SO
ION RESUL
1.014
1.708
0.00
0.07
1.016
1.776
723.215
728.297
5.082
82
87
81
82
83
543
9
0
9.00
1.00
T5
1.014
1.757
0.00
0.02
728.855
735.436
6.781
85
89
83
84
85.25
545.25
10
0
10.00
1.50
1.017
1.823
-0.00
•0.05
735.791
742.073
6.282
87
91
84
85
86.75
546.75
8
0
8.00
2.00
1.017
1.813
-0.00
-0.04
743.976
750.282
6.306
88
92
85
88
87.75
547.75
8
30
6.50
3.00
1.017
1.777
-0.00
-0.00
0
0
0
0
0
0
0
0
480
0
0
0.00
4.00
0.000
0.000
0.00
0.00
Y error (v» prior Y) *"
2.0%
c
* mutt b« no greater than +/- 0.02
** must ba no graatar than +/• 0.20
"• must ba no graatar than +/- 5%
Orifice:
front leak check
back laak cheek
X
X
-------
Date
Calibrated By
Number of Rum
REFEREM
Meter Y 1.016
Vw.Wt
Vw.fin
Vw, total
Pb
tw
Tw+460
DRY GJ
Prevtou»Y 1.016
Vm, toft
Vm.fin
Vm, total
Tdii
Tdif
Tdol
Tdof
Td.avg
Td+460
Time, min
Time, sec
Time Total
dH
CAUBRA7
Y
dH@
Y tolerence from avg *
dH® tol. from avg »*
AVERAGE Y
AVERAGE dH®
03-Sep-«7
MMILBOUR
3
CE TEST Ml
RUN1
388.4
373.864
5.404
29.77
84
544
"kS METER -
335.123
340.601
5.478
86
86
86
86
86
546
15
0
15.00
0.40
ION RESUi:
1.016
1.685
0.00
0.00
1.016
1.686
;NE
RUN 2
373.844
378.247
5.383
29.77
83.5
543.5
340.601
346
5.399
86
85
86
85
85.5
545.5
14
48
14.80
0.40
r°
1.016
1.689
0.00
-0.00
Meter Box Number
MB* ^/n
RUN 3
379.247
384.346
5.099
29.77
83
543
346
351.11
5.11
85
85
85
85
85
545
14
0
14.00
0.40
1.017
1.683
•0.00
0.00
RUN 4
0
0
0
29.77
0
460
0
0
0
0
0
0
0
0
460
0
0
0.00
2.00
0.000
0.000
1.02
1.69
M5-9
RUNS
0
0
0
29.77
0
460
0
0
0
0
0
0
0
0
460
0
0
0.00
3.00
0.000
•0.000
1.02
1.69
Y error (v» prior Y) ***
0.0%
* must be no greater than +/- 0.02
•• must be no greater than +/- 0.20
*** must be no greater than +/- 5%
Orifice:
front leak check
back leak check
Y
Y
-------
DRY GAS METER AND ORIFICE CALIBRATION
CONTROL BOX NO MB-10
DATE: 12MAR97
Hd CH2O)
INITIAL WTM
FINAL WTM
INITIAL DGM
FINAL DGM
TEMP. WTM (F)
TEMP. DGM (F)
TEST TIME (MIN.)
*******************
NET VOLUME WT
NET VOLUME DO
Y
H@
RUN1
0.50
744.467
757.734
653.193
667.139
73.0
81.0
32.4
***********
13.267
13.946
0.964
1.683
BAROMETRIC PRESS. 29.50 IN. HG.
PERFORMED BY : R. GEPHART
RUN 2
0.75
758.780
770.224
668.257
680.310
74.0
84.0
23.1
***********
11.444
12.053
0.965
1.721
RUN 3
1.00
770.733
782.364
680.852
693.138
74.0
86.0
20.5
**********
11.631
12.286
0.966
1.743
RUN 4
1.50
783.592
• 795.014
694.428
706.511
74.0
87.0
16.5
************
11.422
12.083
0.965
1.754
RUN 5
2.00
795.766
807.315
707.301
719.509
74.0
88.0
14.5
***********
11.549
12.208
0.966
1.763
RUN 6
4.00
809.495
822.785
721.813
735.856
74.0
89.0
12.0
:*******
13.290
14.043
0.963
1.820
AVERAGE Y - 0.965
ACCEPTABLE Y RANGE -
AVERAGE H@ - 1.747
ACCEPTABLE dH@ RANGE =
0.945 TO
1.547 TO
Y - (Vw x Pb x (Td + 460)) / (Vd (Pb + (dHd /13.6)) x (Tw + 460)
H@ = 0.0317 x Hd / (Pb (Td + 460)) x ((Tw + 460) x time) / Vw)*2
0.985
1.947
-------
O PACIFIC ENVIRONMENTAL SERVICES, INC.
Central Park West
5001 South Miami Boulevard, P.O. Box 12077
Research Triangle Park, North Carolina 27709-2077
(919) 941-0333 FAX: (919) 941-0234
Posttest Dry Gas Meter Calibration Form (English Units)
Pretest Calibration Factor
System Vacuum Setting, (in Hg)
Reference Meter Correction Factor
Date: 8/22/97 Pbar, in Hg
0.965
6
1.004
29.90 Calibrator:
GG
Meter Box No.
MB-10
AH= 1.9
Trial
1
2
3
Duration
(min)
15
15
15
Dry Gas Meter
Initial
(ft3)
168.592
181.101
191.728
Final
(ft3)
180.101
191.728
203.498
Net
(ft3)
11.509
10.627
11.77
Initial, Inlet
(°F)
90
90
90
Final, Inle
(°F)
90
90
90
Avg. Inlet
(°F)
90
90
90
Initial, Outlet
(°F)
90
90
90
Final, Outlet
(°F)
90
90
90
Avg. Outlet
(°F)
90
90
90
Trial
1
2
3
Reference Meter
Gas Volume
Initial
(ft3)
347.479
358.341
369.176
Final
(ft3)
358.341
369.176
380.031
Net
(ft3)
10.862
10.835
10.855
Meter Temperature
Initial
(°F)
80
80
80
Final
(°F)
80
80
80
Avg.
(°F)
80
80
80
Meter Box
Correction
Factor
Y
0.961
1.038
0.939
Reference
Orifice Press
AH@
(in. H2O)
2.04
2.05
•2.05
10 08227.XLS
Posttest
2/26/98
-------
fcurv v»c;
5001 South Miami Boulevard, P.O. Box 1207
Research Triangle Park, North Carolina 27709-207
(919) 941-0333 FAX: (919) 941-023
Initial Dry Gas Meter Calibration Form (English Units)
Date:
8/19/97
in Hg
30.20 Calibrator. T. McDonald
Meter Box No.
RMB-11
AH = 0.5
Trial
1
2
3
Trial
Duration
(min)
15
15
15
Dry Gas Meter
Gas Volume
Initial
(ft3)
231.840
237.828
Final
(ft3)
237.828
243.880
Net
(ft3)
5.988
6.052
0.000
Meter Temperatures
Initial, Inlet
(°F)
81
82
Final, Inlet
(°F)
81
79
Avg. Inlet
(°F)
81
80.5
#DIV/OI
Initial, Outlet
CF)
78
80
inal, Outle
(°F)
78
78
Avg. Ou
(°F)
78
79
#DIV/(
Trial
1
2
3
Reference Meter
Gas Volume
Initial
(ft3)
257.881
263.670
Final
(ft3)
263.67
269.541
Net
(ft3)
5.789
5.871
0.000
Meter Temperature
Initial
(°F)
78
76
Rnal
(°F)
79
76
Avg.
(°F)
78.5
76
#DIV/OI
Meter Box
Correction
Factor
Y
0.967
0.976
#DIV/0!
Reference
Orifice Press
AHC
(in. H2O)
1.91
1.84
#DIV/0!
AH= 1.8
Trial
1
2
3
Trial
Duration
(min)
10
10
Dry Gas Meter
Gas Volume
Initial
(ft3)
244.055
251.377
Final
(ft3)
251.377
258.770
Net
(ft3)
7.322
7.393
0.000
Meter Temperatures
Initial, Inlet
(°F)
85
84
Final, Inlet
(°F)
80
84
Avg. Inlet
(°F)
82.5
84
#DIV/0!
Initial, Outlet
(°F)
79
79
inal, Outle
(°F)
79
79
Avg. 0
(°F
7£
7£
#D\\
Trial
1
2
3
Reference Meter
Gas Volume
Initial
(ft3)
269.71
276.902
Final
(ft3)
276.902
284.146
Net
(ft3)
7.192
7.244
0.000
Meter Temperature
Initial
(°F)
76
76
Final
(°F)
76
76
Avg.
(°F)
76
76
#DIV/0!
Meter Box
Correction
Factor
Y
0.987
0.986
#DIV/0!
Reference
Orifice Press
AH0
(in. H2O)
1.96
1.93
#DIV/0!
AH = 3.0
Trial
1
2
3
Trial
Duration
(min)
10
10
Dry Gas Meter
Gas Volume
Initial
(ft3)
258.770
268.038
Final
(ft3)
268.038
277.350
Net
(ft3)
9.268
9.312
0.000
Meter Temperatures
Initial, Inlet
(°F)
88
90
Final, Inlet
(°F)
83
86
Avg. Inlet
m
85.5
88
#DIV/0!
Initial, Outlet
CF)
80
81
inal, Outle
(°F)
79
80
Avg.
('
7
8
#D
11 08197.XLS
10/22/97
-------
PACIFIC ENVIRONMENTAL SERVICES. INC.
Central Park West
5001 South Miami Boulevard, P.O. Box 12077
Research Triangle Park, North Carolina 27709-2077
(919) 941-0333 FAX: (919) 941-0234
Posttest Dry Gas Meter Calibration Form (English Units)
Meter Box No. MB-11
Dry Gas Meter No.
Orifice Manometer Setting, dH (in w.c. 2.5
System Vacuum Setting, (in Hg) 2.5
Date:
Calibrated by:
Barometric Pressure, in. Hg
Pretest Calibration Factor
10/13/97
MAD
29.83
0.987
Trial
1
2
3
Trial
Duration
(min)
6.5
7.5
6
Dry Gas Meter
Gas Volume
Initial
(ft3)
56.145
61.57
67.712
Final
(ft3)
61.57
67.712
72.705
Net
(ft3)
5.425
6.142
4.993
Meter Temperatures
Initial, Inlet
(°F)
75
78
83
Final, Inle
(°F)
78
78
87
Avg. Inlet
(8F)
76.5
78
85
Initial, Outlet
(°F)
74
76
77
Final, Outlet
en
79
78
75
Avg. Outlet
CF)
75
77
76
Trial
1
2
3
Reference Meter
Gas Volume
Initial
(ft3)
45.604
51.088
57.3
Final
(ft3)
51.088
57.3
62.309
Net
(ft3)
5.484
6.212
5.009
Meter Temperature
Initial
(°F)
78
79
79
Final
(°F)
79
79
80
Avg.
(°F)
78.5
79
79.5
Meter Box
Correction
Factor
T
1.007
1.010
1.007
Reference
Orifice1 Press
Delta-H@
(in. H2O)
2.01
2.09
2.05
AVERAGE:
% Change:
1.0080
2.13%
2.049
-------
PACIFIC ENVIRONMENTAL SERVICES. INC.
Posttest Dry Gas Meter Calibration Form (English Units)
Central Park West
5001 South Miami Boulevard, P.O. Box 12077
Research Triangle Park, North Carolina 27709-2077
(919) 941-0333 FAX: (919) 941-0234
Reference Meter Calibration Factor 1.004
System Vacuum Setting, (in Hg) 7
Pretest Calibration Factor
0.987
Date:
8/22/97.
in Hg
29.90 Calibrator: GG
Meter Box No.
RMB-11
AH= 1.9
Trial
1
2
3
Duration
(min)
15
15
15
Dry Gas Meter
Initial
(ft3)
993.836
1005.384
1016.948
Final
(ft3)
1005.384
1016.948
1028.471
Net
(ft3)
11.548
11.564
11.523
Initial, Inlet
(°F)
92
92
94
Final, Inle
(T)
92
92
94
Avg. Inlet
<°F)
92
92
94
Initial, Outlet
CF)
92
92
94
Final, Outlet
(°F)
92
92
94
Avg. Outlet
(°F)
92
92
94
Trial
1
2
3
Reference Meter
Gas Volume
Initial
(ft3)
409.91
420.904
431.874
Final
(ft3)
420.904
431.874
442.814
Net
(ft3)
10.994
10.97
10.94
Meter Temperature
Initial
(°F)
80
80
80
Final
CF)
80
80
80
Avg.
(°F)
80
80
80
Meter Box
Correction
Factor
y
0.973
0.969
0.973
Reference
Orifice Press
AHO
(in. H2O)
1.99
2.00
2.00
10/21/97
-------
CM
OL
O)
0)
l/l
(V
VISIBLE EMISSIONS
met the specifications of Fe<£rtiiffirin^^ qualified as a visible
emissions evaluator.'Majdm^'.^^^^^Wf,^^^!^ smoke did not exceed
7.5% opacity and no sing^^rror/exceed^ ^'jpactywas incurred during the
certification test conducj^fy/Eastern Teffic#faso;-i',!-\
^y7 r^g&-\t:--':. .^ i'-^r?t-V^:^- -\2S7158
/>^v~w^ 7^tt^US== : :.-•: :* '.} r-.^^:.; ^-^i^-jfta^,
Progimm Manager
DalcoTIwuc
-------
APPENDIX F
FIELD TESTING PARTICIPANTS
-------
-------
FIELD TESTING PARTICIPANTS
Name
Michael Toney
Mike Maret
Marc Hamilton
Tommy Thompson
Arthur Daughtery
Allen Bass
Barry Rayfield
Jay Morgan
David Goshaw
Tom McDonald
Mike Dickerson
Affiliation
USEPA, Emission Measurement Center
Pacific Environmental Services, Inc..
DEECO"
DEECO"
DEECO"
DEECO3
DEECO3
DEECO
DEECO3
Atlantic Technical Services, Inc.3
Atlantic Technical Services, Inc.3
Responsibility
Work Assignment Manager
Project Manager
Site Leader/Console Operator
Site Leader/Console Operator
Console Operator
Console Operator
Sample Recovery
Sample Recovery
Visible Emissions Observer
Console operator
Console operator
Subcontractor to Pacific Environmental Services, Inc.
-------