United States         Office of Air Quality
Environmental Protection   Planning and Standards
Agency            Research Triangle Park, NC 27711
                                       EPA - 454/R-00-023b
                                       April 2000
     Air
   &EPA
Hot Mix Asphalt Plants
Kiln Dryer Stack
Manual Methods Testing
Asphalt Plant B
Gary, North Carolina
Volume 2 of 2
                  T/r^i
                   ,  *  \  \ J i m.
                '/ "i
                " '•* ^£7~: •
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                         FINAL REPORT

EMISSIONS TEST AT AN ASPHALT CONCRETE PRODUCTION PLANT:
         ASPHALT PLANT "B" - CARY, NORTH CAROLINA
                         VOLUME II OF II
                           APPENDIX C
                           APPENDIX D
                           APPENDIX E
                           APPENDIX F
                     EPA Contract No. 68D70069
                      Work Assignment No. 2-09
                           Prepared for:

                    Mr. Michael L. Toney (MD-19)
                      Work Assignment Manager
                       SCGA, EMC, OAQPS
                 U.S. Environmental Protection Agency
                   Research Triangle Park, NC 27711
                          September 1999
                      p:\i529\finrpt\"B"\mm08119A.wpd
                           Submitted by

             PACIFIC ENVIRONMENTAL SERVICES, INC.
                    5001 S. Miami Blvd., Suite 300
                        Post Office Box 12077
                 Research Triangle Park, NC 27709-2077
                           (919)941-0333
                        FAX (919) 941-0234    y s CnvhwimerrtH Protection Agency

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                                  DISCLAIMER

      This document was prepared by Pacific Environmental Services, Inc. (PES) under EPA
Contract No. 68D70069, Work Assignment No. 2-09.  This document has been reviewed
following PES' internal quality assurance procedures and has been approved for distribution.
The contents of this document do not necessarily reflect the views and policies of the U.S. EPA.
Mention of trade names does not constitute endorsement by the EPA or PES.
                                         11

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                          TABLE OF CONTENTS


VOLUME I                                                          Page

1.0   INTRODUCTION	1-1

2.0   SUMMARY OF RESULTS 	2-1

     2.1   OXYGEN AND CARBON DIOXIDE MEASUREMENTS 	2-1

     2.2   PCDDs/PCDFs MEASUREMENTS	2-1
           2.2.1  Baghouse Inlet - Asphalt Production with RAP  	2-5
           2.2.2  Baghouse Outlet- Asphalt Production with RAP	2-9
           2.2.3  Baghouse Inlet - Asphalt Production without RAP	2-13
           2.2.4  Baghouse Outlet - Asphalt Production without RAP 	2-17

     2.3   PARTICULATE MATTER AND METALS MEASUREMENTS  	2-17
           2.3.1  Baghouse Inlet - Asphalt Production with RAP  	-.	2-17
           2.3.2  Baghouse Outlet- Asphalt Production with RAP	2-25
           2.3.3  Baghouse Inlet - Asphalt Production without RAP	2-25
           2.3.4  Baghouse Outlet - Asphalt Production without RAP 	2-34

     2.4   DETERMINATION OF VISIBLE EMISSIONS 	2-34

3.0   PROCESS DESCRIPTION	3-1

4.0   SAMPLING LOCATIONS	4-1

     4.1   BAGHOUSE INLET SAMPLING LOCATION 	4-1
     4.2   BAGHOUSE OUTLET SAMPLING LOCATION 	4-1

5.0   SAMPLING AND ANALYSIS PROCEDURES	5-1

     5.1   LOCATION OF MEASUREMENT SITES AND
           SAMPLE/VELOCITY TRAVERSE POINTS  	5-1
     5.2   DETERMINATION OF STACK GAS VOLUMETRIC
           FLOW RATE	5-1
     5.3   DETERMINATION OF DRY MOLECULAR WEIGHT
           AND EMISSION CORRECTION FACTORS	5-1
     5.4   DETERMINATION STACK GAS MOISTURE CONTENT 	5-2
                                   111

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                      TABLE OF CONTENTS (Continued)
VOLUME I                                                            Page

      5.5   DETERMINATION OF POLYCHLORINATED DIBENZO-P-DIOXINS
           AND POLYCHLORINATED DIBENZOFURANS	5-2
      5.6   DETERMINATION OF PARTICULATE MATTER AND METALS 	5-4
      5.7   DETERMINATION OF PLUME OPACITY	5-8

6.0    QUALITY ASSURANCE/QUALITY CONTROL PROCEDURES
      AND RESULTS	6-1

      6.1   CALIBRATION OF APPARATUS  	6-1
           6.1.1   Barometers	6-1
           6.1.2   Temperature Sensors 	6-1
           6.1.3   Pilot Tubes	6-1
           6.1.4   Differential Pressure Gauges	6-2
           6.1.5   Dry Gas Meter and Orifice	6-2

      6.2   ON-SITE MEASUREMENTS 	6-3
           6.2.1   Measurement Sites	6-3
           6.2.2   Velocity Measurements	6-5
           6.2.3   Flue Gas Sampling	6-5
           6.2.4   Moisture	6-5
           6.2.5   Method 23/Method 29	6-6

      6.3   ANALYSES	6-6
           6.3.1   Method 23 Analyses 	6-6
           6.3.2   Method 29 Analyses 	6-9

APPENDIX A      PROCESS DATA

APPENDIX B      RAW FIELD DATA

           Appendix B.I  Raw Field Data  Baghouse Inlet
           Appendix B.2  Raw Field Data  Baghouse Outlet
                                    IV

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                      TABLE OF CONTENTS (Concluded)


VOLUME II

APPENDIX C      ANALYTICAL DATA

           Appendix C.I  Analytical Data Method 5 Particulate Matter
           Appendix C.2  Analytical Data Method 23 PCDDs/PCDFs
           Appendix C.3  Analytical Data Method 29 Multiple Metals

APPENDIX D      COMPUTER SUMMARIES

           Appendix D.I  Computer Summaries  Baghouse Inlet  Method 23 & 29
           Appendix D.2  Computer Summaries  Baghouse Outlet Method 9, 23 & 29

APPENDIX E      QA/QC DATA AND CERTIFICATIONS

APPENDIX F      FIELD TESTING PARTICIPANTS

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                         LIST OF TABLES
VOLUME I                                                    Page

TABLE 2.1  EMISSIONS SAMPLING TEST LOG
         ASPHALT PLANT "B" - GARY, NC 	2-3

TABLE 2.2  PCDDs/PCDFs EMISSIONS SAMPLING AND EXHAUST GAS
         PARAMETERS
         ROTARY DRUM DRYER - BAGHOUSE INLET
         ASPHALT PRODUCTION WITH RAP
         ASPHALT PLANT "B" - CARY, NC 	2-6

TABLE 2.3  PCDDs/PCDFs CONCENTRATIONS AND EMISSION RATES
         ROTARY DRUM DRYER - BAGHOUSE INLET
         ASPHALT PRODUCTION WITH RAP
         ASPHALT PLANT "B" - CARY, NC 	2-7

TABLE 2.4  PCDDs/PCDFs CONCENTRATIONS AND 2378 TOXIC EQUIVALENT
         CONCENTRATIONS ADJUSTED TO 7 PERCENT OXYGEN
         ROTARY DRUM DRYER - BAGHOUSE INLET
         ASPHALT PRODUCTION WITH RAP
         ASPHALT PLANT "B" - CARY, NC 	2-8

TABLE 2.5  PCDDs/PCDFs EMISSIONS SAMPLING AND STACK GAS
         PARAMETERS
         ROTARY DRUM DRYER - BAGHOUSE OUTLET
         ASPHALT PRODUCTION WITH RAP
         ASPHALT PLANT "B" - CARY, NC 	2-10

TABLE 2.6  PCDDs/PCDFs CONCENTRATIONS AND EMISSION RATES
         ROTARY DRUM DRYER - BAGHOUSE OUTLET
         ASPHALT PRODUCTION WITH RAP
         ASPHALT PLANT "B" - CARY, NC 	2-11
                               VI

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                     LIST OF TABLES (Continued)
VOLUME I                                                   Page

TABLE 2.7   PCDDs/PCDFs STACK GAS CONCENTRATIONS AND 2378 TOXIC
          EQUIVALENT STACK
          GAS CONCENTRATIONS ADJUSTED TO 7 PERCENT OXYGEN
          ROTARY DRUM DRYER - BAGHOUSE OUTLET
          ASPHALT PRODUCTION WITH RAP
          ASPHALT PLANT "B" - GARY, NC 	2-12

TABLE 2.8   PCDDs/PCDFs EMISSIONS SAMPLING AND STACK GAS
          PARAMETERS
          ROTARY DRUM DRYER - BAGHOUSE INLET
          ASPHALT PRODUCTION WITHOUT RAP
          ASPHALT PLANT "B" - GARY, NC 	2-14

TABLE 2.9   PCDDs/PCDFs CONCENTRATIONS AND EMISSION RATES
          ROTARY DRUM DRYER - BAGHOUSE INLET
          ASPHALT PRODUCTION WITHOUT RAP
          ASPHALT PLANT "B" - GARY, NC 	2-15

TABLE 2.10  PCDDs/PCDFs CONCENTRATIONS AND 2378 TOXIC EQUIVALENT
          STACK
          GAS CONCENTRATIONS ADJUSTED TO 7 PERCENT OXYGEN
          ROTARY DRUM DRYER - BAGHOUSE INLET
          ASPHALT CONCRETE PRODUCTION WITHOUT RAP
          ASPHALT PLANT "B" - GARY, NC 	2-16

TABLE 2.11  PCDDs/PCDFs EMISSIONS SAMPLING AND STACK GAS
          PARAMETERS
          ROTARY DRUM DRYER - BAGHOUSE OUTLET
          ASPHALT PRODUCTION WITHOUT RAP
          ASPHALT PLANT "B" - GARY, NC 	2-18

TABLE 2.12  PCDDs/PCDFs CONCENTRATIONS AND EMISSION RATES
          ROTARY DRUM DRYER - BAGHOUSE OUTLET
          ASPHALT PRODUCTION WITHOUT RAP
          ASPHALT PLANT "B" - GARY, NC 	2-19
                              VII

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                     LIST OF TABLES (Continued)
VOLUME I                                                    Page

TABLE 2.13 PCDDs/PCDFs CONCENTRATIONS AND 2378 TOXIC EQUIVALENT
         CONCENTRATIONS ADJUSTED TO 7 PERCENT OXYGEN
         ROTARY DRUM DRYER - BAGHOUSE OUTLET
         ASPHALT CONCRETE PRODUCTION WITHOUT RAP
         ASPHALT PLANT "B" - CARY, NC 	2-20

TABLE 2.14 PARTICULATE/METALS EMISSIONS SAMPLING
         AND INLET GAS PARAMETERS
         ROTARY DRUM DRYER - BAGHOUSE INLET
         ASPHALT PRODUCTION WITH RAP
         ASPHALT PLANT "B" - CARY, NC 	2-21

TABLE 2.15 PARTICULATE MATTER CONCENTRATIONS AND
         EMISSION RATES
         ROTARY DRUM DRYER - BAGHOUSE INLET
         ASPHALT PRODUCTION WITH RAP
         ASPHALT PLANT "B" - CARY, NC 	2-22

TABLE 2.16 METALS CONCENTRATIONS AND EMISSION RATES
         ROTARY DRUM DRYER - BAGHOUSE INLET
         ASPHALT PRODUCTION WITH RAP
         ASPHALT PLANT "B" - CARY, NC 	2-23

TABLE 2.17 PARTICULATE/METALS EMISSIONS SAMPLING AND
         STACK GAS PARAMETERS
         ROTARY DRUM DRYER - BAGHOUSE OUTLET
         ASPHALT PRODUCTION WITH RAP
         ASPHALT PLANT "B" - CARY, NC 	2-26

TABLE 2.18 PARTICULATE MATTER CONCENTRATIONS AND
         EMISSION RATES
         ROTARY DRUM DRYER - BAGHOUSE OUTLET
         ASPHALT PRODUCTION WITH RAP
         ASPHALT PLANT "B" - CARY, NC 	2-27

TABLE 2.19 METALS CONCENTRATIONS AND EMISSION RATES
         ROTARY DRUM DRYER - BAGHOUSE OUTLET
         ASPHALT PRODUCTION WITH RAP
         ASPHALT PLANT "B" - CARY, NC 	2-28

                              viii

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                     LIST OF TABLES (Continued)
VOLUME I

TABLE 2.20  PARTICULATE/METALS EMISSIONS SAMPLING AND
          STACK GAS PARAMETERS
          ROTARY DRUM DRYER - BAGHOUSE INLET
          ASPHALT PRODUCTION WITHOUT RAP
          ASPHALT PLANT "B" - GARY, NC 	
                                                  Page
                                                  2-30
TABLE 2.21
PARTICULATE MATTER CONCENTRATIONS AND
EMISSION RATES
ROTARY DRUM DRYER - BAGHOUSE INLET
ASPHALT PRODUCTION WITHOUT RAP
ASPHALT PLANT "B" - GARY, NC  	
                                                            2-31
TABLE 2.22  METALS CONCENTRATIONS AND EMISSION RATES
          ROTARY DRUM DRYER-BAGHOUSE INLET
          ASPHALT PRODUCTION WITHOUT RAP
          ASPHALT PLANT "B" - GARY, NC 	
                                                  2-32
TABLE 2.23
PARTICULATE/METALS EMISSIONS SAMPLING
AND STACK GAS PARAMETERS
ROTARY DRUM DRYER - BAGHOUSE OUTLET
ASPHALT PRODUCTION WITHOUT RAP
ASPHALT PLANT "B" - GARY, NC  	
                                                            2-35
TABLE 2.24  PARTICULATE MATTER CONCENTRATIONS AND
          EMISSION RATES
          ROTARY DRUM DRYER - BAGHOUSE OUTLET
          ASPHALT PRODUCTION WITHOUT RAP
          ASPHALT PLANT "B" - GARY, NC 	
                                                  2-36
TABLE 2.25
METALS CONCENTRATIONS AND EMISSION RATES
ROTARY DRUM DRYER-BAGHOUSE OUTLET
ASPHALT PRODUCTION WITHOUT RAP
ASPHALT PLANT "B" - GARY, NC 	
                                                            2-37
                               IX

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                     LIST OF TABLES (Continued)
VOLUME I                                                    Page

TABLE 3.1   PLANT OPERATING CONDITIONS
          ASPHALT PLANT "B" - GARY, NC	3-3

TABLE 3.2   ASPHALT MIX SPECIFICATIONS
          ASPHALT PLANT "B" - CARY, NC	3-5

TABLE 3.3   FUEL SPECIFICATIONS
          ASPHALT PLANT "B" - CARY, NC	3-5

TABLE 3.4   SPECIFICS OF PLANT OPERATION
          ASPHALT PLANT "B" - CARY, NC	3-6
TABLE 5.1   SAMPLING LOCATIONS, TEST PARAMETERS, AND
          TEST METHODS SUMMARY
          ASPHALT PLANT "B"-CARY, NC	5-2
TABLE 6.1   SUMMARY OF TEMPERATURE SENSOR CALIBRATION DATA
          ASPHALT PLANT "B" - CARY, NC	6-2

TABLE 6.2   SUMMARY OF PITOT TUBE DIMENSIONAL DATA
          ASPHALT PLANT "B" - CARY, NC	6-4

TABLE 6.3   SUMMARY OF DRY GAS METER AND ORIFICE
          CALIBRATION DATA
          ASPHALT PLANT "B" - CARY, NC	6-5

TABLE 6.4   SUMMARY OF METHOD 237 METHOD 29 FIELD SAMPLING
          QA/QC DATA
          ASPHALT PLANT "B" - CARY, NC	6-7

TABLE 6.5   SUMMARY OF METHOD 23 STANDARDS RECOVERY
          EFFICIENCIES
          ASPHALT PLANT "B" - CARY, NC	6-8

TABLE 6.6   SUMMARY OF METHOD 29 ANALYSIS QC DATA
          LAB CONTROL SPIKES
          ASPHALT PLANT "B" - CARY, NC	6-11

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                     LIST OF TABLES (Continued)
VOLUME I                                                    Page

TABLE 6.7  SUMMARY OF METHOD 29 ANALYSIS QC DATA
          POST DIGESTION MATRIX SPIKES RUN NO. R-O-M29-1
          ASPHALT PLANT "B" - GARY, NC	6-12

TABLE 6.8  METHOD 29 SERIAL DILUTION ANALYSIS QC DATA
          RUNNOR-0-M29-1
          ASPHALT PLANT "B" - GARY, NC	6-13

TABLE 6.9  METHOD 29 DUPLICATE ANALYSIS QC DATA
          RUN NO. R-O-M29-2
          ASPHALT PLANT "B" - GARY, NC	6-14

TABLE 6.10  METHOD 29 METHOD BLANK ANALYSIS QC DATA
          ASPHALT PLANT "B" - GARY, NC	6-15

TABLE 6.11  METHOD 29 FIELD AND REAGENT BLANK ANALYSIS
          QC DATA
          ASPHALT PLANT "B" - GARY, NC	6-16

TABLE 6.12  METHOD 29 MERCURY SPIKE ANALYSIS QC DATA
          ASPHALT PLANT "B" - GARY, NC	6-17

TABLE 6.13  METHOD 29 MERCURY FIELD BLANK ANALYSIS QC DATA
          ASPHALT PLANT "B" - GARY, NC	6-18
                               XI

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                                 LIST OF FIGURES


VOLUME I                                                                      Page

Figure 1.1    Key Personnel and Responsibility for Testing - Asphalt Plant "B", Gary, NC . 1-3

Figure 1.2    Sampling Locations - Asphalt Plant "B", Gary, NC	1-4


Figure 4.1    Baghouse Inlet Sampling Location - Asphalt Plant "B", Gary, NC	4-2

Figure 4.2    Baghouse Inlet Point Locations - Asphalt Plant "B", Gary, NC	4-3

Figure 4.3    Baghouse Outlet Sampling Location - Asphalt Plant "B", Gary, NC	4-4

Figure 4.4    Baghouse Outlet Point Locations - Asphalt Plant "B", Gary, NC	4-5


Figure 5.1    Method 23 Sample Train Schematic - Asphalt Plant "B" Gary, NC  	5-3

Figure 5.2    Method 29 Sample Train Schematic - Asphalt Plant "B", Gary, NC  	5-5

Figure 5.3    Method 29 Sample Recovery Scheme (Sample Fractions 1-4)
             Asphalt Plant "B", Gary, NC  	5-6

Figure 5.4    Method 29 Sample Recovery Scheme (Sample Fraction 5)
             Asphalt Plant "B", Gary, NC	5-7
                                         XII

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   APPENDIX C




ANALYTICAL DATA

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      Appendix C.I




      Analytical Data




Method 5 Particulate Matter

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--     /1.   .1 *-   ••-*
(   7 PACIFIC ENVIRONMENTAL SERVICES, INC.
                                                        3708 Mayfair Street. Suite 202
                                                        Durham. North Carolina 27707
                                                                (919)493-3538
                                                              Fax: (919) 493-7779
                              SAMPLE ANALYTICAL  DATA FORM
          Plant
^ fortifier
                                    "8"
Run number 1-7$-Q-i
Sample  location 	
Relative humidity 	;
Density of acetone (pa)
                      O,
                                gf\6AQmSe-
                                                                           g/ml
Sample
type
Acetone rinse
filter (s)
Sample
identifiable
tlh'Tt
vw-6\3 . m -23
Liquid level marked
and/or container sealed

Acetone rinse container number
Acetone rinse volume  (V_,_) 	
                                               7G7-9
                                           ml
Acetone blank residue concentration  (C  )
Wa = CaVawPa=  <<>
Date and time of  wt
Date and time of  wt
                                                                 CLOOOO
                                                     Gross  wt
                                                     Gross  wt

                                                                  O. &OOO
                                                                            nig
                                  Average gross wt
                                            Tare wt
                        Less acetone  blank wt (W_)
                                                 a
      Weight of particulate in  acetone rinse (m  )
 Filter (s) container number    ggcW  VJQ   VV-fS
 Date and time of wt       Q^o5"    Gross wt
 Date and time of wt    Qf?*?^?   Iffi^    Gross wt
                                  Average gross wt
          IbLrtW  t^  fr-~*Z $  F.\W  fl^ -fivl  Tare wt
          Weight of particulate on filter(s) (m~)
           Weight of particulate in acetone rinse
                  Total weight of particulate (m  )
 Note;   In no  case should a blank residue >0.01 mg/g or 0.001% of
 the weight  of acetone used be  subtracted from the sample weight.
           Remarks
                 Signature of  analyst
                 Signature of  reviewer
                                    r
                       WASHINGTON. OC. • RESEARCH THIANSLE PARK. NC • LOS ANGELES. CA • CINCINNATI. OH

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1 PACIFIC ENVIRONMENTAL SERVICES, INC.
                                                                       3708 Maytalr Street. Suite 202
                                                                       Durham, North Carolina 27707
                                                                                (919) 493-3536
                                                                             Fax:(919)493-7779
                               SAMPLE ANALYTICAL DATA FORM
         Plant
Sample location 	
Relative  humidity 	;
Density of acetone (pa)
                                                    Run number
                                            0
Sample
type
Acetone rinse
filter(s)
Sample
identifiable
flu -74
W*ft-   V\A -3
Acetone rinse volume (V___) l44T-f
Acetone blank residue concentration (C_)

a a aw a ~^~~
Date and time of wt ^/^/^ To"1? Gross wt
Date and time of wt "l/?6r?3- £)^3T Gross wt
Average gross wt
Tare wt
Less acetone blank wt (W )
a —
Weight of particulate in acetone rinse (in )
r— ~"
Filter(s) container number V^t-ldt (WA">-0\9
Date and time of wt ^/?4f^ IQ&>~ Gross wt
Date and time of wt ^T^*? tfa T Gross wt
Average gross wt
Tare wt
Weight of particulate on filter(s) (mf)
Weight of particulate in acetone rinse
Total weight of particulate (m_)
ml
Ci - O CoO ofa/g
Ci . OOCC pg
WLfc^KF 4i
VO^S^oo V9
\0\.0l9^ Big

Q .Cxyt) mg
6-0246 ^a

C . STZ-A-I- jrfg

0.^43 i*g
0 . 4-S$9 m'a
n.0134 X«
0.01 mg/g or 0.001% of
the weight of acetone used be subtracted from the sample weight.
          Remarks
                 Signature of  analyst
                 Signature of  reviewer
                        WASHINGTON. DC. • RESEARCH TRIANGLE PMW. NC • LOS ANQELES. CA • CMOWMTI. OH

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i  ,' PACIFIC ENVIRONMENTAL SERVICES, INC.
                                                                  3708 Maytair Street. Suite 202
                                                                  Durham, North Carolina 27707
                                                                          (919) 493-3536
                                                                        Fax:(919)4837779
                              SAMPLE ANALYTICAL DATA FORM
          Plant
                                               Run number
Sample location 	
Relative humidity 	
Density of acetone (p_)
                                                                          g/ml
Sample
type
Acetone rinse
filter (s)
Sample
identifiable
\d~\c
KV-O?V W-il
Liquid level marked
and/or container sealed

Acetone rinse container number
                                                             \A) - IQ
Acetone rinse volume  (V   )  	
                        c|W  - -  —•—
Acetone blank residue concentration (Ca)
                                        £1
                                                                            ml
                                                               QjQOQO
Wa =
                Ca Vaw
           Date and time of wt
           Date and time of wt
                                          Gross wt
                                          Gross wt
                                                      Ufc.fldll
                                 Average gross wt
                                           Tare wt
                       Less acetone blank wt (Wa)
                                                GL
     Weight of particulate in  acetone rinse (m,)
                                 T^ |     v      A
Filter(s)  container number
Date and time of wt _
Date and time of wt
                                                      103.
                                                                           ma
                                                                   . poop
                                       	 Gross wt
                      	 Gross wt
                                  Average gross wt
                  tVU-UJT F.lW l*-<™      Tare wt
          Weight of particulate on filter(s) (m-)
           Weight of particulate in acetone rinse
                  Total weight of particulate (m  )
                                                                (63.
                                                                (65.
                                                                          /fig
           Note;   In no case should a blank residue >0.01 mg/g  or 0.001% of
           the weight  of acetone used be  subtracted from the sample weight.
           Remarks
                Signature of analyst
                Signature of reviewer
                                VIA
                       WASHINGTON. DC • RESEARCH TRIANGLE PARK. NC • LOS ANGELES. CA • CINCINNATI. OH

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                                        \
   PACIFIC ENVIRONMENTAL SERVICES, INC.
                                                                  3708 Mayfair Street. Suite 202
                                                                  Durham, North CareUna 27707
                                                                          (919)493-3536
                                                                       Fax:(919)493-7779
                             SAMPLE ANALYTICAL DATA FORM
r
          Plant
Sample location 	
Relative  humidity 	
Density of acetone (pa)
                      a,
                                               Run number
                                                                - X- JL
                                        a.
Sample
type
Acetone rinse
filter(s)
Sample
identifiable
'Ealfr WM1-
   j&g
          Note;   In no case should a blank residue  >0.01 mg/g or  0.001% of
          the  weight of acetone  used be subtracted  from the sample weight.
Remarks
•W
                           AM?,
                                     ^cJi  IftA
                Signature of analyst
                Signature of reviewer
                      WASHINGTON. QC. • RESEARCH TRIANQLE PARK. NC • LOS ANQELES. CA « CMCMNATI. OH

-------
17 PACIFIC ENVIRONMENTAL SERVICES, INC.
                                                                 3708 Mayfalr Street. Suite 202
                                                                 Durham. North Carolina 27707
                                                                         (919)493-3536
                                                                       Fax:(919)493-7779
                             SAMPLE ANALYTICAL DATA FORM
Plant
                                 niarr ''£• "
                                                Run number Tl-'^'T-'Z,
Sample  location 	
Relative humidity 	-
Density of acetone (p  )
                                          \(\Ji
                                     tT
                                      Q .
                                                                 g/ml
Sample
type
Acetone rinse
filter(s)
Sample
identifiable
^_U VYM1
|ftH, \OG*, ^tW N
Liquid level marked
and/or container sealed
-n-
         Acetone rinse container number
         Acetone rinse volume  (V.,,.)
                                 clW  ~~    ~~     —
         Acetone blank residue concentration (C.
                                                                   ml
W  = C  V   D  =  ( fc
*  A     A  £tX*7 ~ SI    *
  A     C*  An  C&

Date and time of  wt
Date and time of  wt
                                   )   ( 64*0 )  (
                                                        o.oooo
                                           Gross wt
                                           Gross wt
                                   Average gross wt
                                            Tare wt
                        Less acetone blank wt  (W  )
      Weight  of particulate in acetone rinse  (m  )
                                                 d
                                                                too.
                                                                          fig
                                                                          **
                                                                  6.0QOO
 Filter(s) container number
 Date and time of wt    °i\n.
 Date and time of wt
                                                    V\M1-
                                                	 Gross wt
                                                    Gross wt
                                           Average gross wt

                   Weight  of particulate on filter(s) (mf)
                    Weight of particulate in acetone rinse
                           Total weight of particulate (m  )
          Note:  In no case should a blank  residue >0.01  mg/g or 0.001%'of
          the weight of  acetone used be subtracted from the sample weight.
          Remarks
               Signature  of analyst
               Signature  of reviewer
                     VWSHINGION. D.C « RESEARCH TRIANGLE PARK. NC • LOS ANGELES. CA • CINCINNATI. OH

-------
(  J PACIFIC ENVIRONMENTAL SERVICES, INC.
                                                         3708 Maytair Street, Suite 202
                                                         Durham, North Carolina 27707
                                                                 (919) 493-3536
                                                              Fax:(919)493-7779
 C
                               SAMPLE ANALYTICAL DATA FORM
Plant
           Sample location 	
           Relative humidity 	
           Density of  acetone d
                                                 "E"
     Run number V, -7^1 -"1 -3
                                                                 g/»l
Sample
type
Acetone rinse
filter(s)
Sample
identifiable
^0.01 mg/g or 0.001% of
            the weight of acetone used be subtracted from the sample weight.
 Remarks
                      \xu
                                                                         of
                 Signature of analyst
                 Signature of reviewer
                        NWkSMINGtON. O.C • RESEARCH TRIANGLE PARK. NC • LOS ANGELES. C* • CMCINNXn. OH

-------
                                      \
17 PACIFIC ENVIRONMENTAL SERVICES, INC.
                                                                3708 Maytair Street. Suite 202
                                                                Durham. North Carolina 27707
                                                                        (919) 493-3536
                                                                      Fax (919) 493-7779
                            SAMPLE  ANALYTICAL DATA FORM
        Plant
Sample  location 	
Relative humidity 	
Density of acetone (p_)
                      cl
                                          "B"   Run number fl- -7A - ^
                                                                        g/ml
Sample
type
Acetone rinse
filter(s)
Sample
identifiable
VJ-CL
vu^-cv^
Liquid level marked
and/or container sealed

Acetone rinse container number 	
Acetone rinse volume  (VM_)  	
                        ow   	~" —~r- L~~—"' ~	
Acetone blank residue concentration (C )
                                        cl
                                                      |)Jo
                                                                              *Jl
                                                               O-O006
Date  and time of wt
Date  and time of wt
                                          (63T
Gross wt
Gross wt
                                                     (6S.ZICO
                                                        e .OQ6Q
                                                        o.ccol
                                                                         7
                                                                         *g
                                                               0.4W
                                  Average gross wt
                                           Tare wt
                       Less acetone blank wt (W )
                                                a
      Weight of particulate in acetone rinse (m )
Filter(s) container number      F> \W  No   tyAQ"3
Date  and time of wt    ^/7.4nT-   t^S^"    Gross wt
Date  and time of wt   flfer ^   6^0.01 mg/g or 0.001% of
the weight of acetone used be subtracted from the  sample weight.
                                                                6. COOL
         Remarks
               Signature of analyst _
               Signature of reviewer
                     WASHINGTON. OR. • RESEARCH TRIANGLE PARK. NC • LOS ANOELE& CA • CINCINNATI. OH

-------
m
>
w


$
                                                    METHOD 5
                                                  TARE HEIGHT
    Project Numbers
                                                       Item Weiahedi
     Dat
     R.H.  (%)
     •MIMHM
     Temi
  (•F)
     Std. Ht,
     Analyst
      ID Number
       j(VL£
3
       •AMkMHM^^H
       V^W
         Field Sample
            Number
1st
2nd
                                  a/.sfl
     !6U9tS
                        ifiS
                                  ^
                                          flj.6016
                                         VMBMlMXMMMBMB^
                                         Q7-30^3
                                                   3rd
4th
                               5th
 Final
Ht. (g)
   Tare
 Ht.  (g)
'V J-, 
                                               SI
                                                                            t5§3^
                                                                                     X
                                                                                    1ST.
                                                                                               Difference
                                                                                                              ?i

-------
        f-  J
                                                   METHOD 5

                                                 TARE WEIGHT
8
m
C»
m
s
>>
Project Humbert
                                                      Item Weiahedi
     Date
     R.H. (%)
     Temp. (*F)
     Std. Wt.
     Analyst
ID Number
          - COT
     -004-
      ^a
           on-
     ^7A
       si
                  Field Sample

                     Number
                (?dv  T-
                    t-
                             0 •
                               1st
                                 6.363T-
                              .36(2,
                                 0-
                                  twj
                                          2nd
                                         0.30(0
                                         Q 44Q-?
                                        ^
                                         0
                                        ZM
3rd
4th
5th
 Final

Wt. (g)
                                                                   0-3608
                                                                       6 .
                                                                         . 36?^
                                                                        6
                                                                       A.3Bl.(
                                                                        6
                                                                                    Tare
Difference

   (ng)
                                                                                                          ^
                                                                                                          fl«l
                                                                                                          en
                                                                                                         _i.

-------
1
5
I
1
1
f»
!
>roject Numl
Date
R.H. (%)
Temp. (*F)
Std. Wt.
Analyst
ID Number
VfPtTt-&i$























>er« ^4G-O64






Field Sample
Number

























$1

~^4-^
0 *&&
iWivi
1st
644*1?
6448<<
6.4441
o
6.<
&
4
























Tare
Wt. (g)





























Difference
(nig)











'












"B
1

-------
W
a:
     •w
    -1

      I  ..£
     \f
       M

      i
      §
      4J
       O
      ?
       Vl
                  3-
                      >

                      5 -»
                      w cr
                      0 6
« o»»
                      S «—
                        in
D Number
                            0^4-
                            ^^
    pr«
                                
-------
II
O
m
m

^
M
                                                       METHOD 5
                                                     FINAL WEIOIT
     Project Number:
                                                           Item Weighed:
                                                   F.lU
      Date
      R.H.
      Std. Wt,
      Analyst
ID Number
     m-s
                   Field  Sample
                      Number
1st
                                             lo-'T
                                        2nd
                                                    l£O. OOOO
3rd
4th
                                                                     ')•
                                 5th
 Final
Wt.  (g)
  Tare
Ht.  (q)
                                                                                               Difference
                                                                                                   (mg)
     JMt-
                     tffe
              <-\6.'X>°4
                                                                        l(6.^<30fr
                                          ^b&
                                                                        661?
                                                    \off. tcffa
          U/T
        .Lt
                                            0.5144-
                                                    6. 4468
                 ca^  VA^W^.  Uctf-<;L-^
      iU,>s T
      ^n:

-------
     Appendix C.2




    Analytical Data




Method 23 PCDDs/PCDFs

-------
                            CASE NARRATIVE
                     Analysis of Samples for the Presence of


            Polychlorinated Dibenzo-p-Dioxins and Dibenzofurans by


     High-Resolution Chromatography / High-Resolution Mass Spectrometry
                                Method 23 (6/93)
             Date:


             Client ID:


             P.O. Number:


             TLI Project Number:
September 18, 1997


Pacific Environmental Services


104-98-0019- & -0020


43085
This report should only be reproduced in full. Any partial reproduction of this report requires permission from
Triangle Laboratories, Inc.
Rev. 05/08/97
                                             Triangle Laboratories, Inc.
                                  801 Capitola Drive             P.O. Box 13485        \
                                  Durham, NC 27713-4411         Research Triangle Park, fie 27709-3485
                                  919-544-5729                 Fax # 919-544-5491
                                                                                      1

-------
Triangle Laboratories, Inc.                                              September 18, 1997
Case Narrative                                                                  43085
Overview

Eight M23 samples were received from Pacific Environmental Services in good condition
on September 03, 1997 at 6.0 °C. The samples were stored in a refrigerator at 4°C.  The
samples and any associated QC samples were extracted and analyzed according to
procedures described in the Triangle Laboratories' Data User's Manual (Rev.  12/92-HK-
2-AH-2/93). Any particular difficulties encountered during the samples' handling by
Triangle Laboratories will be discussed in the QC Remarks section below.  Results
reported relate only to the items tested.

Quality Control Samples

A laboratory method blank, identified as the TLIM23 Blank, was prepared along with the
samples.

Laboratory control spike (LCS) and laboratory control spike duplicate (LCSD) samples
were extracted and analyzed along with the samples. A report summarizing the analyte
recoveries and relative percent differences for these samples is included in the data
package.

Quality Control Remarks

This release of this particular set of Pacific Environmental Services analytical data by
Triangle Laboratories was authorized by the Quality Control Chemist who has reviewed
each sample data package individually following a series of inspections/reviews.  When
applicable, general deviations from acceptable QC requirements are identified below and
comments are made on the effect of these deviations upon the validity and reliability of the
results. Please consult Triangle Laboratories' Data User's Manual for further details.
Specific QC issues associated with this particular project are:

Sample Preparation Laboratory: As per client request, the impinger samples are to be
archived and not analyzed.

Samples O-M23-1,  O-M23-2, I-M23-1, I-M23-2, and I-M23-3  had larger than
normal XAD traps, requiring several Soxhlet apparatus.

Mass Spectrometry: None

Data Review: Most of the samples exhibit severe matrix-related problems. There are
shifts in the retention times and severe quantitative interferences.  As a result, several
samples have elevated detection limits, out-of-ratio labeled standards, and labeled

-------
Triangle Laboratories, Inc.                                              September 18, 1997
Case Narrative                                                                   43085
standards that are below the QC criteria of 10:1 signal-to-noise. The final reports have
been flagged accordingly.  Please refer to the data flags for further details and possible
effects on data quality.

Other Comments:. Any analytes found in the TLIM23 Blank are detected at a level equal
to or less than the Target Detection Limit. This level of contamination is acceptable as per
TLI guidelines.

Sample Calculations:

Analyte Concentration

The amount of any analyte is calculated using the following expression.

                                  Ao  *  Qp
                     Amt{0)= 	
                              Ap*RRF(0)*W

Where:

Amt (o) is the amount of a given analyte,

AC is the integrated current for the characteristic ions of the analyte,

Ap is the integrated current of the characteristic ions of the corresponding internal
standard,

Qp represents the amount of internal standard added to the sample before extraction,

RRF(o) is the mean analyte relative response factor from the initial calibration (ICal) and,

W is the sample weight or volume (W = 1 for M23)

The amount is expressed in nanograms (ng) or picograms (pg).


 Detection Limits

The detection limit reported for a target analyte that is not detected or presents an analyte
 response that is less than 2.5 times the background level is calculated by using the
 following expression.  The area of the analyte is replaced by the noise level measured in a
 region of the chromatogram clear of genuine GC signals multiplied by an empirically
 determined factor.  The detection limits represent the maximum possible concentration of
 a target analyte that could be present without being detected.

-------
Triangle Laboratories, Inc.                                               September 18, 1997
Case Narrative                                                                   43085
                             2 * 2.5 * (F * H) * QP
                     DL(a)= 	
                               Ap*RRF(a) *W

Where:

DL(a) is the estimated detection limit for a target analyte,

2.5 is the minimum response required for a GC signal,

F is an empirical number that approximates the area to height ratio for a GC signal.  This
number is 3.7 for both the DB-5 GC column and the DB-225 GC column,

H is the height of the noise

Ap is the integrated current of the characteristic ions of the corresponding internal
standard,

Qp represents the amount of internal standard added to the sample before extraction,

RRF(0) is the mean analyte relative response factor from the initial calibration (ICal) and,

W is the sample weight or volume

The detection limit is expressed in nanograms (ng) or picograms (pg).

Other sample calculations may be found in the Triangle Laboratories Data User's Manual.


Data Flags

In order to assist with data interpretation, data qualifier flags are used on the final reports,
as discussed in Triangle Laboratories' Method 23 Data User's Manual.  Please note that all
data qualifier flags are subjective and are applied as consistently as possible. Each flag has
been reviewed by  two independent Chemists and the impact of the data qualifier flag on
the quality of the data discussed above. The most commonly used flags are:

A 'B' flag is used to indicate that an analyte has been detected in the laboratory method
blank as well as in an associated field sample. The 'B' flag will be used only when the
concentration of analyte found in the sample is less than 20 times that found in the
associated blank.  This flag denotes possible contribution of background laboratory
contamination to the concentration or amount of that analyte detected in the field sample.
Under Triangle Laboratories guidelines, a laboratory blank is acceptable if the tetra-

-------
Triangle Laboratories, Inc.                                               September 18,1997
Case Narrative                                                                  43085
through hepta-CDD/CDF levels are all below the target detection limits (TDLS) or if the
contamination levels are less than 5% of the levels detected in the associated field samples.
If these conditions are satisfied or if the blank is unable to be reextracted, the
interpretation of the contamination levels relative to the samples should be as follows: 1)
analyte quantitations should be considered valid if the level of blank contamination is less
than five percent of the level detected in the field sample, 2) analyte quantitations should
be considered estimated if the analyte level in the sample is five to twenty times the level
of the analyte in the blank, or 3) analytes whose level in a sample is the same as or less
than five times the level detected in the associated blank should be considered present
likely due to laboratory contamination and not native to the sample.

An 'E' flag is used to indicate that an PCDF peak has eluted at the same time as the
associated diphenyl ether (DPE) and that the DPE peak intensity is ten percent or more of
the PCDF peak intensity. Total PCDF values are flagged 'E' if the total DPE contribution
to the total PCDF value is greater than ten percent. All PCDF peaks that are significantly
influenced by the presence of DPE peaks are  quantitated with EMPC values, regardless of
the isotopic abundance ratio. These EMPC values are most likely overestimated due to
the DPE contribution to the peak area.

An 'I' flag is used to indicate labeled standards have been interfered with on the GC
column by coeluting, interferent peaks.  The interference may have caused the standard's
area to be overestimated. All quantitations relative to this standard, therefore, may be
underestimated.

A 'PR' flag is used to indicate that a GC peak is poorly resolved. This resolution problem
may be seen as two closely eluting peaks without a reasonable valley between the peak
tops, overly broad peaks, or peaks whose shapes vary greatly from a normal distribution.
The concentrations or amounts reported for such peaks are most likely overestimated.

A 'Q' flag is used to indicate the presence of QC ion instabilities caused by quantitative
interferences. Affected analytes may be overestimated or underestimated as a result of this
interference. A peak is flagged 'Q' only if it is affected by a QC ion deviation greater than
20% full scale as determined relative to the labeled standard against which it is
quantitated. Total PCDF/PCDF quantitations will  be flagged 'Q' if the interferences affect
ten percent or more of the total PCDD/PCDF peak areas.

An 'RO' flag is used to indicate that a labeled standard has an ion abundance ratio that is
outside of the acceptable QC limits, most likely due to a coeluting interference.  This may
have caused the percent recovery of the standard to be overestimated.  All quantitations
versus this standard, therefore, may be underestimated.

A 'U' flag is used to indicate that a specific (2,3,7,8-substituted) isomer cannot be
resolved from a large, coeluting interferent GC peak. The specific isomer is reported as

-------
Triangle Laboratories, Inc.                                               September 18,1997
Case Narrative                                                                   43085
not detected as a valid concentration/amount cannot be determined. The calculated
detection limit, therefore, should be considered an underestimated value.

A 'V flag is used to indicate that, although the percent recovery of a labeled standard may
be below a specific QC limit, the signal-to-noise ratio of the peak is greater than ten-to-
one. The standard is considered reliably quantifiable. All quantitations derived from the
standard are considered valid as well.
By our interpretation, the analytical data in this project are valid based on the guidelines
of EPA Method 23 (6/93) and Triangle Laboratories' Method 23 Data User's Manual.
Any specific QC concerns or problems have been discussed in the QC Remarks section of
this case narrative with emphasis on their effect on the data.  Should Pacific
Environmental Services have any questions or comments regarding this data package,
please feel free to contact our Project Scientist, Amy Boehm, at (919) 544-5729, ext.
268.
For Triangle Laboratories, Inc.,


Report Preparation                        Quality Control
 Sheila A. Lee-Lewis                          1
 Report Preparation Chemist                Report Preparation Chemist
 The total number of pages in the data package is :

-------
                     TRIANGLE LABORATORIES, INC.

                LIST OF CERTIFICATIONS AND ACCREDITATIONS
ENVIRONMENTAL

American  Association  for  Laboratory  Accreditation. Certification  pending.   Certificate
Number 0226-01. Accreditation for technical competence in Environmental Testing.(Including
Waste  Water, Sol/Haz Waste, Pulp/Paper, and Air Matrices)   Parameters  are AOX/TOX,
Volatiles, Pesticides, PCB's. BNA's, and Dioxin/Furan. Method 1613 for Drinking Water.

State of Alabama, Department of Environmental Management Expires December 31, 1997.
Laboratory I.D. #40950. Dioxin in drinking water.

State of Alaska, Department of Environmental Conservation. Expires December 21, 1997.
Certificate number OS-00397. Dioxin in drinking water.

State of Arizona, Department of  Health Services.   Expires May 26, 1998. Certificate
#AZ0423. Drinking Water for Dioxin, Dioxin in WW and S/H Waste.
 State of Arkansas, Department of Pollution Control and Ecology.   Expires February 18,
 1998. Pulp/paper, soil, water, and Hazardous Waste for Dioxin/Furan; AOX/TOX.

 State of California, Department of Health Services.  Expires August 31, 1999. Certificate
 #1922. Selected Metals in Waste Water; Volatiles, Semi-volatiles, and Dioxin/furan in WW and
 Sol/Haz Waste. Dioxin in drinking water.

 State  of  Connecticut, Department  of Health Services.  Expires  September 30, 1997.
 Registration # PH-0117. Dioxin in drinking water.

 Delaware Health and  Social Services. Expires December 31, 1997. Certificate #NC  140.
 Dioxin in drinking water.

 Florida Department of Health and Rehabilitative Services. Expires June 30, 1998.Dioxin in
 DW. Drinking Water ID HRS# 87424.  Metals, Extractable Organics (GC/MS), Pesticides/PCB's
 (GC) and  Volatiles (GC/MS)  in Environmental  Samples.   Environmental water ID HRS#
 E87411.

 Hawaii Department of Health. Expires March 1, 1998. Dioxin  in drinking water. "Accepted"
 status for regulatory purposes .
 Revised 9/18/97 RM

 Printed 9/18/97

-------
Idaho Department of Health and Welfare.  Expires November 30, 1997. Dioxin in drinking
water.

State of Kansas, Department of Health and  Environment  Expires January 31, 1998.
Environmental Analyses/Non potable Water and  Solid and Hazardous Waste. Method 1613
for drinking water. ID #'s - Drinking water and/or pollution control - E-215. Solid or Hazardous
Waste-E-1209.

Commonwealth of Kentucky, Department for Environmental Protection. Expires December
 31, 1997. ID#90060. Dioxin in drinking water.

Maryland Department of Health and  Mental Hygiene.   Expires September 30, 1997.
Certification #235.  Drinking water by Method 1613A.

State of Michigan, Department of Public Health. Expires March 31, 1998. Drinking water by
Method  1613.

Mississippi State Department of Health. No expiration date.. Dioxin in drinking water.

Montana Department of Health and Environmental Services.  Expires December 31, 1997.
Dioxin in drinking water.

State of New Jersey, Department of Environmental Protection and Energy. Extended by
state. Temporary certificate until December 31,1997. ID #67851. BNAs and Volatiles. Dioxin in
drinking water.

State of New Mexico,  Environment Department. Certification pending. Dioxin in drinking
water.

 New York State Department of Health. Expires June 30,  1997.  ID #11026. Environmental
Analyses of non-potable Water, Solid and Hazardous Waste. Method 1613 in DW.

 State of North Carolina, Department of Environment Health  and Natural  Resources
 Expires August 31,  1999. Certificate # 37751.  Dioxin in drinking water.

 State of North Carolina,  Department of Env onment,  Health, and  Natural Resources,
 Division of Environmental Management  Expires December 31, 1997. Certificate # 485.
 Metals,  pesticides & PCBs, semi-volatiles and volatiles; TCLP.

 North  Dakota State  Department  of  Health  and Consolidated  Laboratories.   Expires
 December 31, 1997. Certificate # R-076. Effective October 4, 1993.  Dioxin in drinking water.
 Revised 9/18/97 RM

 Printed 9/18/97                                                                          5

-------
Oklahoma Department of Environmental Quality.  Expires October 31, 1997.  Laboratory
#9612. Dioxin by 1613A, 8290 and 8280.

State of South Carolina, Department of Health and Environmental Control.  Expires June
30, 1997. Certificate number #99040001 (drinking water). Expires August 31, 1999. Certificate
number #99040002 (other parameters). Dioxin/Furans, BNA, Volatiles, and PCBs/pesticides
under Clean Water Act, 2,3,7,8-TCDD for Drinking Water, and Organic extractables for Solid
and Hazardous Waste.

State of Tennessee. Department of Environment and Conservation. Expires February 5,
1999. ID #02992.  Method 1613 Drinking water only.

U.S. Department of Agriculture Soil Permit  Expires September 30,  2001. Permit No. S-
3790. Under the authority  of the Federal Plant Pest Act, permission is granted to receive
foreign soil samples for use in laboratory analysis.

U.S. Army Corps of Engineers. Expires November 30, 1997. Validated to perform methods
8280 & 8290 for Lockbourne Landfill Site Investigation, Defense Distribution Depot Projects,
and assorted projects for the USAGE North Pacific Division Laboratory.

U.S. EPA  Region V. Expires  November 14, 1999. Dioxin in drinking water.

U.S.  EPA Region VIII, for the State of Wyoming. Expires November 13, 1997.  Dioxin in
drinking water.

State of Utah, Department of Health. Expires December 31, 1997. Certificate Number E-166.
Certification for the following parameters:  Semi-Volatiles and Volatiles under RCRA; Volatiles
under Clean Water Act; Dioxin/furans by Method 8280; Drinking water  for Dioxin by Method
 1613; Metals including Mercury and Microwave Digestion.

 Commonwealth of Virginia, Department of General Services,  Division of Consolidated
 Laboratory Services. Expires June 30, 1998. ID # 00341. Dioxin in drinking water.

 State of Washington, Department of Ecology. Expires September 1998. Lab Accreditation
 Number C067.  Scope of Accreditation applies to water analyses for Polychlonnated Dibenzo-
 p-dioxins  and Polychlonnated Dibenzofurans, BNA Extr (Semivolatile) Organics and Purgeable
 (Volatile) Organics.

 State of Washington, Department of Health. Expires April 30, 1998.  Dioxin in drinking water.
  Labl.D.  129

 State of West Virginia, Department of Health. Expires December 31, 1997. Certificate No.
 9923(C). Dioxin in drinking water.
 Revised 9/18/97 RM

 Printed 9/18/97

-------
State of Wisconsin,  Department  of  Natural  Resources.  Expires  August 31,  1998.
Laboratory  ID  Number  999869530.  Certification for  the  following categories of  Organics:
Purgeable, Base/Neutral, Acid, PCBs, and Dioxin. Expires  November 14, 1999. Laboratory ID
999869530. Dioxin in drinking water.

PHARMACEUTICAL

Drug Enforcement Agency (DEA). Expires  November 30, 1997.  Registration  number
RT01195835. Controlled substance registration for schedules 1,2,3,3N,4,5.

N.C. Department of Human Resources. Expires October 31, 1997. Registration number NC-
PT 0000 0031. North Carolina  controlled  substances registration. Application submitted for
renewal.

Food & Drug Administration (FDA)  Registration. Expires June 1998.  ID #'s  001500
1053481. Annual registration of drug  establishment. Annual registration of drug establishment.

OTHER

Clinical Laboratory Improvement Amendments (CLIA) Registration. Expires May 30, 1999.
ID  # 34D0705123.  Department of  Health  & Human  Services,  Health Care  Financing
Administration.

U.S.  EPA  Large Quantity Hazardous Waste  Generator.  No expiration date.   EPA  ID
#NCD982156879. Permit indicates that the laboratory is a large generator of hazardous waste.

North Carolina Radioactive Materials License.  Expires April  30  1998. License No. 032-
0954-1. License authorizes the licensee to receive, acquire, own, possess, transfer,  import and
use such radioactive materials as designated.

 North Carolina General License for Radiation Protection. No. expiration date. License No.
032-875-OG.  The general license  applies only to radioactive material contained  in devices
which have been manufactured and labeled in accordance with specific  requirements.
 Revised 9/18/97 RM
 Printed 9/18/97
                                                                                     10

-------
DOCUMENT
  CONTROL
           Triangle Laboratories, Inc.
     801 Capitola Drive      P.O. Box 13485
     Durham, NC 27713-4411     Research Triangle Park, NC 27709-3485
     919-544-5729         Fax * 919-544-5491
                              11

-------
PACIRC ENVIRONMENTAL SERVICES. INC.
                         Central Park WeSTJ
    5001 South Miami Boulevard, P.O. Box 12077
Research Triangle Park, North Carolina 27709-2077
           (919)941-0333 FAX: (919) 941-0234
                                                Chain of Custody Record
Project Num
s4 13-004
Project Name
US EPA EMC Asphalt Cement, ^t/. Asphalt Vt^ur "g
Samplers:
Dickerson, McDonald. Thompson, Hamiliton
Date
8/27/97
8/27/97
8/27/97
8/27/97
8/27/97
8/27/97
8/27/97
8/27/97
8/27/97
8/28/97
8/28/97
8/28/97
8/28/97
8/28/97
8/28/97
8/28/97
8/28/97
8/28/97
Time
0945
0945
0945
0945
0945
0945
0945
0945
0945
0845
0845
0845
0845
0745
0745
0745
0745
0745
Field Sample ID
l-M23-1-AceATol
I-M23-1 -Filter
I-M23-1-XAD
l-M23-1-lmp
O-M23-1-Ace/Tol
O-M23-1 -Filter
O-M23-1-XAD
O-M23-1-lmp(1/2)
O-M23-1-lmp(2/2)
l-M23-2-Ace/Tol
l-M23-2-Filter
I-M23-2-XAD
l-M23-2-lmp
O-M23-2-Ace/Tol
O-M23-2-Filter
O-M23-2-XAD
O-M23-2-lmp (1/2)
O-M23-2-lmp (2/2)
Relinquished by: (Signature)
Relinquished by: (Signature)
Relinquished by: (Signature)
<
Dateffime
AT-/1
Datemme
Date/Time
Sample Description
Acetone / Toluene Rinse
Filter
XAD Trap
BH Impinger Contents
Acetone/ Toluene Rinse
Filter
XAD Trap
BH Impinger Contents
BH Impinger Contents


Acetone / Toluene Rinse
Filter
XAD Trap
BH Impinger Contents
Acetone/ Toluene Rinse
Filter
XAD Trap
BH Impinger Contents
BH Impinger Contents
Received by: (Signature)
Received by: (Signature)
Received for lab by: (Signature)

Analysis Requested

PCDD
-
•
•

.
•
•


.
•
*

•
•
.


PCDF
•
-
•

•
-
•


-
•
*

*
•
•



























































Relinquished by: (Signature)
Relinquished by: (Signature)






































Date/Time
Datemme
REMARKS

Remarks



ARCHIVE



ARCHIVE
ARCHIVE



ARCHIVE



ARCHIVE
ARCHIVE
Received by: (Signature)
Received by: (Signature)

|Page: of

-------
PACIFIC ENVIRONMENTAL SERVICES. INC.I
                          Central Park West
    5001 South Miami Boulevard. P.O. Box 12077
Research Triangle Park, North Carolina 27709-2077
           (919) 941-0333  FAX: (919) 941-0234
                                                Chain of Custody Record
Project Num
8413-004
Project Name
US EPA EMC Asphalt Cement, . Asphalt TiAMg
Samplers:
Dickerson, McDonald, Thompson, Hamilton
Date
8/29/97
8/29/97
8/29/97
8/29/97
8/29/97
8/29/97
8/29/97
8/29/97
8/29/97
8/29/97
8/29/97
8/29/97
8/29/97
8/29/97
8/29/97
8/29/97
8/29/97
8/29/97
Time
0745
0745
0745
0745
0745
0745
0745
0745
0745
0745
0745
0745
0745
0745
0745
0745
0745
0745
Field Sample ID
-M23-3-Ace/Tol
l-M23-3-Filter
-M23-3-XAD
l-M23-3-lmp
O-M23-3-Acem>l
O-M23-3-Filter
O-M23-3-XAD
O-M23-3-lmp (1/2)
O-M23-3-lmp (2/2)
O-M23-FB-Ace/Tol
O-M23-FB-Filter
O-M23-FB-XAD
O-M23-FB-lmp
M23-RB - Acetone
M23-RB - Filters
M23-RB-XAD
M23-RB-Toluene
M23-RB - Water
Relinquished by: (Signature)
7£/&>^^
-------
Custody Seal : Present/Intact Sample Seals: Present
Chain of Custody : Present Container...: Intact
Sample Tags : Absent
Sample Tag Numbers: Not Listed on Chain of Custody
SMO Forms : N/A '
Ice Chest ICE PACKS Temp 6.0 C
TLI Project Number 43085 ,
Client: PES03 - Pacific Environmental Servic
Date Reoelved 09/03/97 1 By /&l)
\ i ITfi //*
I f ff ^/ ~
Carrier and Number | TIM MCDONALD
1 Book I
1 1
1 "I 1


CLI Number 	 Client Sample ID 	 Matrix) To LJ
nR/H:CPM. 	 Client COC ID • Location j Date/
	 |
\B To STORAGE) To LAB
'Init Date/Init Date/Init
i
181-55-1A 0-M23-1 -FILTER FILTERJ L,$( \
0-M23-X-FILTER C02 j ^^ \1|CI?P»
LB1-5S-1B 0-M23-1-XAD XAD|
0-M23-1-XAD C02 |
181-55-1C 0-M23-1-IMP IMP)
O-H23-1-IMP C02 j
1
it I -55 -ID 0-M23-1-IMP IMP)
0-M23-1-IMP C02 j
j
1
181-5S-1E O-M23-1-ACB/TOL ACE/TOL|
- 0-M23-1-ACB/TOL C02 j I
1
I • ' { ' 1



1 1
L11-5S-2A O-M23-2-FILTER FILTER) \
^ O-M23-2-FILTER C02 j I
I 1
1
1*1-55-28 0-M23-2-XAD XAD|
~~ O-M23-2-XAD C02 j
j
L81-5S-2C 0-M23-2-IMP FH/RINSE)
O-M23-2-IMP C02 j
j
1
[81-5S-2D O-M23-2-IMP BH/RINSE)
O-M23-2-IMP C02 j
p81-S5-2E O-M23-2-ACE/TOL IMPINGERJ
•» 0-M23-2-ACE/TOL C02 j
L81-S5-3A O-M23-3-FILTER FILTER)
' O-M23 -3 -FILTER C02 |
1
1
.81-55-3B 0-M23-3-XAD XAD)
f- O-M23-3-XAD C02 j
j
L81-5S-3C 0-M23-3-IMP FH/RINSEJ (
0-M23-3-IMP C02 j I
I \
L81-55-3D 0-M23-3-IMP BH/RINSE) \j
O-M23-3-IMP C02 j
1





/











\

/l^-
i
1
\
h&D
/
•
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To STORAGE
Date/Init














| To LAB
Date/Init




'





'



To STORAGE
Date/Init






t







| To LAB
Date/Init














To STORAGE
Date/Init














| DISPOSED
Date/Init














Receiving Remarks:
Archive Remarks:
=Form Revised 05/27/1997 -- Page 1 OF 3=

-------

Custody Seal i Present/Intact Sample Seals: Pr
Chain of Custody : Present Container. . . : In
Sample Taga i Absent
Sample Tag Numbers: Not Listed on Chain of Custody
SMO Forma : N/A '
LB LABORATORIES, IKC. -- LOO IN RECORD/CHAIN OF
esent TLI
tact Cli

U *
Project Number 43085 , | Book
ent": PES03 - Pacific Environmental Service* j
| 181
i
Date Received | 09/03/97 *Ytf /~liSl*~ £ 	 \V*3*
i i fa &f7r4s&2s& \
Ice Chest ICE PACKS Temp 6.0 C Carrier and Number j TIM MCDONALD ^ j 55
i i i
TLI Number 	 Client Sample ID 	 4 	 Matrix
nR/H-CPM Client COC ID 	 * Location 	

181-5S-3B 0-M23-3-ACE/TOL IMPINGER
s. O-M23-3-ACE/TOL C02
181-SS-4A O-M23-FB-FILTER FILTER
) O-M23-FB-FILTER C02
181-55-4B 0-M23-FB-XAD XAD
> 0-M23-FB-XAD C02
181-S5-4C O-M23-FB-IMP FH/RINSE
0-M23-FB-IMP C02
181-S5-4D 0-M23-FB-ACE/TOL BH/RINSE
1 O-M23-FB-ACE/TOL C02
1S1-55-SA 1-M23-1-FILTER FILTER
> 1-M23-1-FILTER C02
181-SS-SB 1-M23-1-XAD XAD
/ 1-M23-1-XAD C02
181-55-5C 1-M23-1-IMP FH/RINSE
1-M23-1-IMP C02
181-5S-5D 1-M23-1-ACE/TOL BH/RINSE
' 1-M23-1-ACE/TOL C02
181-5S-6A 1-M23-2-FILTER FILTER
1-M23-2-FILTER C02
181-55-6B 1-M23-2-XAD XAD
1-M23-2-XAD C02
181-55-6C 1-M23-2-IMP FH/RINSE
1-M23-2-IMP C02
181-55-6D 1-M23-2-ACB/TOL BH/RINSE
" lrM23-2-ACE/TOL C02
181-55-7A 1-M23-3-FILTER FILTER]
1-M23-3-FILTER C02 |
| To LAB
Date/Init
L/
1/V/











I
I
* I










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/
To STORAGE | To LAB
Date/Init j Date/Init
j
f* >^>













SuSfD
/t
1
1
1
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^\}JiV
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Date/Init







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....
1 	 1




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Date/Init





	 1
1 	 1


	




To STORAGE
Date/Init





	
t
	
	 1




1
| To LAB
Date/Init






1 	 1
| 	 1






To STORAGE
Date/Init
•



.... 	 	 	


| 	 1






DISPOSED
Date/Init




, 	 	 - — I
I 	 1
1 	 1

	 1





Receiving Remarks:
Archive Remarks:











=Form Revised OS/27/1997 -- Page 2 OF 3=

-------
•TRIANGLE LABORATORIES,  INC. -- IAAS  in  Km_umj/I.IUMII vr
Custody Seal : Present/Intact Sample Seals: Present
Chain of Custody : Present Container...: Intact
Sample Tags : Absent
Sample Tag Numbers: Not Listed on Chain of Custody
SMO Forms : N/A '
TLI Project Number 43085 ,
Client: PES03 - Pacific Environmental Services
1 1 SI /
Date Received | 09/03/97 1 &{///? /^ss&Z***.
i i iS*\ 1 J^r *^
1 Book
1
| 181
^ 	
^ 1 P«9«
i // wi • i
Ice Chest ICE PACKS Temp 6.0 C Carrier and Number | TIM MCDONALD " V 1 55
PL! Number 	 Client Sample ID 	 t 	 Matrix
nR/H:CPM. 	 Client COC ID. .. * Location 	

L81-SS-7B 1-M23-3-XAD XAD
1-M23-3-XAD C02
181-5S-7C 1-M23-3-IMP FH/RINSE
1-M23-3-IMP C02
L81-5S-7D 1-M23-3-ACE/TOL BH/RINSE
1-M23-3-ACE/TOL C02
L81-55-8A . M23-RB-FILTER FILTER
M23-RB-FILTER C02
LB1-5S-8B M23-RB-XAD XAD
M23-RB-XAD C02
181-5S-8C M23-RB -ACETONE FH/RINSE
M2 3 -RB- ACETONE C02
L81-SS-8D M23-RB-HATER BH/RINSE
M23-RB-HATER C02
L81-55-8B M23-RB-TOLUENE IMPINGER
> M2 3 -RB- TOLUENE C02






1 To LAB To STORAGE
Date/Init Date/Init
I
LD tf






M/







\
\
J
/


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| To LAB
Date/Init
£D


,


w&







To STORAGE
Date/Init














| To LAB
Date/Init














To STORAGE
Date/Init






I
•»






| To LAB
Date/Init














To STORAGE
Date/Init














| DISPOSED
Date/Init














Receiving Remarks:
Archive Remarks:
          =Form Revised 05/27/1997 -- Page  3  OF 3=

-------
                          TRIANGLE LABORATORIES,  INC.
                  SAMPLE TRACKING AND  PROJECT MANAGEMENT FORM
   	ADMINISTRATIVE INFORMATION	
   TLI  Proj#:  43085-      Samples:  8            TurnAround.: 14 Day(s)
   Prod Code:  D23061      Matrix.:  M23Train    Hold Time..: 30 Day(s)
   DetectLim:  0.05 ng     Type...:  A            Start Date.: 09/03/97
                           Recvd..:  09/03/97    Ship By....: 09/15/97
                                                 DWL Due Dt.: 09/10/97

   Analyte List.: tetra-octa PCDDs/PCDFs

   Method	: Method 23:Tetra-Octa (Tol Combined)
   Client Proj..: S413-004
   Client	: Pacific Environmental  Services (PES03)
   P.O. No	: 104-98-0019 &  -0020           Collect Dt/Tm: SeeCOC
   Contact	: Frank Meadows                 Phone	: 919-941-0333
   Proj .  Mgr.  . .  . : Amy J. Boehm                  Fax	: 919-941-0234
                                                 Sample Origin: NC
   	SPECIAL  INSTRUCTIONS / QA REQUIREMENTS	
    Prep Project: 03803                      Prespike Standard: USF-CS
                                             Prespike Amount..: 4.Ong
                                             Extraction Exp...: 09/26/97
   -------------------------- REPORTING REQUIREMENTS
    Reporting Format: Report Option II

    See MILES for Instructions/Communications.
    Completed by: _ _ _  DATE:

    Reviewed by: _ ^£2 _  DATE:  T/T^/er      (PMGT0197
Triangle Laboratories, Inc.® Analytical Services Division
801 Capitola Drive • Durham, North Carolina 27713                                 Printed:417:21 09/02/WE
Phone: (919) 544-5729 • Fax: (919) 544-5491                                                  IY

-------
Date:  09/04/97
rime:  20:29
 Sample
 •  crd TLI_Number..  Customer.Sample.Id

 000    TLI  Blank    TLI M23 Blank

 001    181-55-1ABE   0-M23-1

 002    1B1-S5-2ABE   0-M23-2

 003    181-55-3ABE   0-M23-3

 004    181-55-4ABD   O-M23-FB

 005    181-55-5ABD   I-M23-1

 006     181-55-6ABD   I-M23-2

 007     181-55-7ABD   I-M23-3

 008     181-55-8ABDE M23-RB

 009    TLI LCS      TLI LCS

010    TLI LCSD     TLI LCSD

••• End of Report •**
 TRIANGLE LABORATORIES,  INC.
Wet Lab MM5/PUF Observations
       Project: 43085
                                                                                                                                                       Page:  1
F.
	 No
0
1
1
1
1
4
4
4
1
0
0
XAD
Color
WHITE
WHITE
WHITE
WHITE
WHITE
WHITE
WHITE
WHITE
WHITE
WHITE
WHITE
Filter Glass Wool PUF
. . Color. . Color 	 Color. . .

WHITE/BRWN WHITE/YELL
WHITE/BRWN WHITE/YELL
WHITE/BRWN WHITE/YELL
WHITE WHITE
WHITE/BRWN WHITE
WHITE/BRWN WHITE
WHITE/BRWN WHITE
WHITE WHITE


. . Odor . . .
NONE
OIL
OIL
OIL
NONE
OIL
OIL
OIL
NONE
NONE
NONE
Air
. . Q . No . Entered . By 	
03803 ADKINS
03803 ADKINS
03083 ADKINS
03803 ADKINS
03803 ADKINS
03803 ADKINS
03803 ADKINS
03803 ADKINS
03804 ADKINS
ADKINS
ADKINS
                                                                Date....   Time..

                                                               09/04  20:29 F

                                                               09/04  20:29 F

                                                               09/04  20:29 F

                                                               09/04  20:29 F

                                                               09/04  20:29 F

                                                               09/04  20:29 F

                                                               09/04  20:29  F

                                                               09/04 20:29 F

                                                               09/04 20:29 F

                                                               09/04 20:29 F

                                                               09/04 20:29 f
                                                                                 .  S

-------
                  TRIANGLh LJ\bUtlAiUriiC£> ur n i r, UNO.

                   PROJECT COMMUNICATION TRACKIN'G FORM
                      TL1 Project Number:
page  _ of   .
Use this form to record all exchanges of information between production units as well as personnel
handling -this project. Decisions, corrective actions and recommendations must also appear on this
                                tracking document
ate





Name


-

Comment / Decision /
Resolution / Action / Observation
? \tfdZ5-
ffl iL | ^T ^y
n t< i< *•
*^\. *V— *^ < * f •* \l ^^
^ • •
' PESOS-Pacific Environmental Services .
0-M23-1-FTLTER
             R r-o j ©o-t. :  -4- 3 O © 5
                  1 a 1  — 55 — 1 A

             PES03-Pacific Environmental  Services
                     O-M23-1-ACE/TOL
                    1 Q I —55— 1 E
            PESOS-Pacitic Environmental  Services
                       O-M23-1-XAD
                   1 © 1 — 5 5— 1 B
                                                                  /
            "PES03-P"acif"ic  tnvironmentai services
                       O-M23-2-XAD
              F» r~o j e»c-t. :  -4-3OS5
                   1 ©1  — 5 5 —2B
                       c  tnvironmental Services
                    0-M23-2-ACE/TOL
                     J^o-t. :  4-3OQ5
                     e1  —55 —2E
                       c  hnvironmentai services
                    O-M23-2-FILTER
              Rt-ojoo-t. :  -4-3OQ5
                   1©1—55—2A

-------
                        PROJECT COMMUNICATION TRACKING FORM
                                                                    page .Z. of
                           TL1 Project Number:
         .            —-             •	                                    -^•~~-^——
     Use this form to record all exchanges of information between production units as well as personnel
   '  handling -this project. Decisions, corrective actions and recommendations must also appear on this
                                     tracking document
Date
Name
Comment / Decision / Resolution / Action / Observation
     ===================================  ~ ~
     PES03-Pacific Environmental Services
              0-M23-3-ACE/TOL
        P r- o j & G ^ : -4- 3 O © 5
            1 © 1 —55—SEE
     PtSQ3-Pacific Environmental  Services
              0-M23-3-FILTER     .   '
       R r-o j ©G-fc. : -4-3 O © 5
            1 ©1 — 5 5 — 3 A
     PES03-Pacitic Environmental  Services
                0-M23-3-XAD
       Rr-oJ^Gt : 4-3O©5
           1  ©1 —55 —SB
                  PES03-Pacific Environmental Services
                            0-M23-FB-XAD
        \
                  1 e 1  — 55 — -4-B

           "PES03-Pacific Environmental Services
                    0-M23-FB-FIITER
              Pr-ojj^o-t. : -4-3OQ5
                   1 e 1 — 55 — ^-A
            PES03-Pacitic Environmental Services
                    O-M23-FB-ACE/TOL
              Rr-ojoo-t :  -4-3OQ5
                   1 e 1 — 55 — 4-D
                                Environmental Services
                           1-M23-1-FILTER
                    R r~ o j o o t : A- 3 O Q 5
                         1e1—55—5A
                   PESOS^-Pacific Environmental SeTvToes
                            1-M23-1-ACE/TOL
                     Pr-oj^ot :  -4-3OQ5
                          1 ©1 —55— 5D

                    PES03-Pacific Environmental  Services
                                1-M23-1-XAD
                      Pr-oj^G-t : -4-3OQ5
                           1 ©1 —55 —SB
                                                                                       20

-------
                      TRIANGLE LABORATORIES OF RTP, INC.

                       PROJECT COMMUNICATION TRACKING FORM
                                                                        page _£__ of  v3
                         TL1 Project Number:
    Use this form to record all exchanges of information between production units as well as personnel
    handling -this project. Decisions, corrective actions and recommendations must also appear on this
                                   tracking document
ate
     Name
Comment / Decision / Resolution / Action / Observation
                        i r ic. mv 1 1 onmenta i  services
                        1-M23-2-FILTER
                          ©c-t- : -4-3O85
                           1 — 55 — ©A
                            c bnvironmentai  Services
                            1-M23-2-XAD
                            eo-t : -£ 3 O Q 5
                       1 e 1 — 55— ©B
                PES03-Pacific Environmental Services
                        1-M23-2-ACE/TOL
                  F1 t-oj eot : -4-3O Q 5
                       1 e  1 — 5 5— ©D
                   F» r-o
                PESO3-Pacific Environmental Services  ,
                           1-M23-3-XAD             1
                           1 — 5S— 7
                               Bwlr
               PES03-Pacific Env"ironmentaT~Serv1ces
                        1-M23-3-FILTER
                 Rr-ojeso-t : -4-3OQ5
                      1 e 1 —55— 7A
                                                                             >
M
(  4>
                 PESOS-Pacific Environmental Sec vices" »
                           M23-RB-XAD              L
                       1 e 1 — 55 — 8B
                PES03-Pacific Environmental
                         M23-RB-FILTER
                       1  e 1 —55— ©A
                "PES03-Pacif1c Environmental Services
                         M23-RB-ACETONE
                            oo-t. = 4-3OQ5
                            1 — 55 — 8C

-------
TRIANGLE LABORATORIES, INC. PAGE 1 OF 2
Dioxin Sample Preparation Tracking & Management Form
Project: 43085 Client: Pacific Environmental Services (PES03)
Solvent (s) /Acid(s) : /0/U^TO
IS Spike: 40 jil oonc: 0.1000 ng/ul •"
SS Spike: ul cone: . nq/ul
MS Spike: 0 ul cone: 0.0000 ng/ul
LCS Spike: 0 pi cone: 0.0000 ng/ul
OPR Spike: 	 20 ul cone: _0.01 	 ng/ul
| | TLI / | GROSS | SAMPLE
|Stt.crd| SAMPLE / CLIENT | HEIGHT | SIZE
| | ID / SAMPLE ID | Before After | g / ml
| I TLI Blank | | I
|000 | TLI M23 Blank ] | | f
| | 181-55-1ABE | | |
|001 | 0-M23-1 | | | J

^ , /*-" , TO- ;
525V I 1 S'Z.VSS | *\£3(\-h i
u<>F x. i use #* i JJSF-/4 i
7. / oZ/^| ij. / ij_ i3$\ $_ / £. 1^1 1
°l /cri ft~l | 3_ /oV /£7 1 £. / ^. /f£7 1
ii = 2s i d_ = lL i JL = L5_ i
•O'/ ng/ul 1 0.6( nq/Mi | fl./ nq/Bi |
VO ul 1 tO ul 1 40 ul 1


1 Chemis
1 Spike
" ID
_ / _ /_ " Exp
	 / 	 / 	 " Dat
	 : 	 " Tim
nq/j»l * Con
ul " Vol

4^. ( . | | /\JJi/ 1 t'yes/Y
/ yfrs^ ^-t^
^ I i * i
| | 181-55-2ABE | | | | , I 1 - x*~N "' 1
1002 | 0-M23-2 | | | I |iXL , , . | 1 /Sj4jX 1
1 _y \/rrr —
| | 181-5S-3ABE | | I 1 / /? 1 1 x-~N 1
|003 1 0-M23-3 | | | | | /_ / .1, , 1 1 fr\ LJJ^ 1
| | 181-55-4ABD | | I 1 X , ^ 1 \ * -"~\ 1
|004 | 0-M23-FB | | III O^-" ~~ ' 1 1 r\l-L£__ \
	 + 	 	 	 . 	 	 	 .....L_+ 	 +. 	 ../OJrrrr...
|Any Le
| ye i/r
|Any L€
	 [.Y.y.
|AnyJL.
1 yea/i
|Any |L
1 yes/
|       | 181-55-5ABD
|005    |
                            I-M23-1
                                                                                                                       |AnyL
|       | 181-S5-6ABD
|006    |
                             I-M23-2
                                                                                          |Any'tL
                                                                                          I  ye^/
        181-55-7ABD
|007
        I
I-M23-3  |
                                                                                                                       |Any|l
|       | 181-55-8ABDE
1008    |
                                     |
                              M23-RB |
                                                                                                                       |Any
       |  TLI  LCS
 |009
                                     |
                             TLI LCS |
                                                                    s.C
                                                                                    ,
                                                                                           |Any\I
  Gross weight of  sample container + sample before/after aliquot removal.
   Comments:
                                         -
                                             r
                                                                   (jof
                                                                                           Initials :
                                                                                                              Date:
                                                                                                                    7,
 I  Initials of both SPIKER AND OBSERVER must be entered.
                                                                             XXXXX -  Gross Height not provided for HATER Sampl
                                                                            	REV 05/27/97 (PSTMF

-------
Project: 43085
Solvent (a)/Acid(s)
Lot Numbers:
IS Spike: 40 Ml
SS Spike: Ml
MS Spike: 0 Ml
LCS Spike: 0 ul
OPR Spike: 	 20 M!
| TLI
;#.crd| SAMPLE /
] ID /
| TLI LCSD
no |
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
TRIANGLE LABORATORIES, INC. PAGE 2 OF 2 )
Dioxin Sample Preparation Tracking & Management Form \
Client: Pacific Environmental Service* (PESO 3) 1
: "Talut^vA- / / Method: Method 23:Tetra-Octa (Tol Combined) Matrix: fffl^ J
^7^1 )B 1 1 Extraction Date: 7 1 ^ I^H \
\
cone: . ng/ul 1 Ln 1 LT\ | 6-A 1 (Chemist 1
cone: 0.0000 na/ul 1 $2^1 1 52.3^3 | 52.35'5 1 1 Spike * t
cone: 0.0000 na/nl 1 OS P J. | UST A\X 1 USF'A 1 1 " ID 1
cone: _0.01_ ng/Ml I _Z / °2/3& 'J: / Z7/JL3! H. 1 £ /$ \ _ / _ /_ 1 ' Expiri
.. . . 	 	 «. 	 + 	 + 9 /^V/^71 ^ 1 OV I<1'^ Q 1 (a 1^1 \ 1 1 \ 'Date 1
/ | GROSS | SAMPLE | _ll = ^ I {!_ = H 1 JL'i5L 1 	 = 	 1 ' Tin« (
CLIENT 1 WEIGHT 1 SIZE I O- ) ng/(il I O-Olnq/ul | 0-i na/ul 1 ng/ul 1 * Conc.l
SAMPLE ID | Before After | a / ml | ^O ul 1 ^Cj ul 1 'fo ul 1 tfl 1 " Vol. 1

1 i 1 1 , ., 1 ^ /-'- 1 ^-X 1 lAnyLeft*
TLI LCSD | | | [ | X. . C_ . L^ ' ^ ' | /SlW^ | |fl%)no |
+ 	 nr. 	 + ^Urrr^- + .. >^.- «.
III! 1 1 1 lAnyLeft)
I 1 1 I 1 1 1 1 yes/no j
1 1 1 1 1 1 1 lAnyLeftj
1 ! 1 1 1 1 1 1 yes/no |
1 1 ! 1 1 1 1 |AnyLeft|
1 1 1 1 1 1 1 1 yes/no 1
1 I 1 1 1 1 1 |AnyLeft|
1 1 I 1 ! 1 1 1 y~/no 1
1 1 1 1 1 I I |Any Leftj
1 1 1 1 1 1 1 1 yes/no |
1 1 1 I 1 1 I |AnyLeft|
1 1 1 1 1 1 1 1 y*s/no 1
1 1 1 1 1 1 1 |Any Left)
lilt 1 1 I 1 yes/no i
1 1 1 1 1 1 1 (Any Left
1 1 1 1 1 1 1 1 yes/no
till | | | |Any Left
1 1 1 1 1 1 1 1 yes/no
Gross weight of sample container + sample before/after aliquot removal.

 Comments:	  	   	
                                                                                           Initials:
Initials of both SPIKER AND OBSERVER must be entered.
                                                                             XXXXX » Gross Height not provided for HATER Samples.
                                                                            	-.l-.-REV OS/27/97  (PSTOF 7)--
                                                                                                                            23

-------
                                                                                                          PAGE 1 OF 2
                                            TRIANGLE LABORATORIES, INC.
                                 DIOXIN SAMPLE EXTRACTION and CLEANUP TRACKING FORM
                                               TLI  Project No.: 43085
Ext Stt.crd
TLI Number
 Enter the procedure  number below into the box at the top of each column to signify the step performed.
 Initial  and  date  each sample for each numbered procedure performed.
                                  %'jfa'l
tt	PROCEDURE	 DETAJ£S (circle)
^JX EXTRACT I ON                    ON   OFF	<£oxhla& / Jar / Sep Funnel  /  Steam Dist / Cont LL / ASE / Waste Dilut:
•(JP SPIKE AFTER EXTRACTION      '*''"
£^U)ADD TRIDECANE               /'
f ^\f ROTOVAP                       4 OtnL
 5) COMBINE                                      _._
ffP DIVIDE /  LIPID DETERMINATION  20%/80V    (SOV/SOVJ) 5mL/20mL    Other_
    SOLVENT EXCHANGE—"—    Q
   i CLEANUP// ,4^>^X6c/1a^-vvw^SP~TGT^ /  DSP 225  /  DSP 115  /  DSP 215  /  DSP 267   /  Other
   > TRANSFER
  10)  ADDITIONAL CLEANUP
  11)  FINAL TRANSFER
                                   Mod. DSP 260  /  DSP 225  /  DSP 115  /  DSP 215  /  DSP  267   /   Other
   Comments:
                                                                                               -Rev 06/24/97  (PSTMF  4

-------
                                                                                                         PAGE 2 OF 2
                                            TRIANGLE LABORATORIES, INC.
                                 DIOXIN SAMPLE EXTRACTION and CLEANUP TRACKING FORM
                                               TLI Project No.: 43085
Ext S#.crd  and
TLI Number
                   i
Enter the procedure number below into the box at the top of each column to signify the step performed.
Initial and date each sample for each numbered procedure performed.

i	PROCEDURE	 DETAILS  (circle)
    EXTRACTION                    ONJ^OFF_  /   DSP  225  /  DSP  115   /  DSP 215  /  DSP 267   /  Other
/fp TRANSFER
10) ADDITIONAL CLEANUP
11) FINAL TRANSFER
                                                        5mL/20mL    Other
                                   Mod. DSP 260  /  DSP 225  /  DSP 115  /  DSP 215  /  DSP 267   /   Other
  Comments:
                                                                                              «Rev 06/24/97 (PSTM? 41 •
                                                                                                                  25

-------
                                                                  PAGE 1 OF
                         TRIANGLE LABORATORIES,  INC.
                        Transfer Chain-of-Custody Form
                                Project 43085

                     Transfer  From:  DWLH5     To: DMS5

                            Initials. .     Date	    Time. . .

              Released by:   JL&        __2./JL/_£Z    /? ; C>~0

              Accepted by:  	    	/	/	    	:	
1 	
MILES. ID
43085-
43085-
43085-
43085-
43085-
43085-
43085-
43085-
43085-
43085-
43085-

-000
-001
-002
-003
-004
-005
-006
-007
-008
-009
-010
TLI
TLI
181
181
181
181
181
181
181
181
TLI
TLI
No 	
Blank
-55-1ABE
-55-2ABE
-55-3ABE
-55-4ABD
-55-5ABD
-55-6ABD
-55-7ABD
-55-8ABDE
LCS
LCSD
Gust .Id 	
TLI M23 Blank
O-M23-1
O-M23-2
O-M23-3
O-M23-FB
I-M23-1
I-M23-2
I-M23-3
M23-RB
TLI LCS
TLI LCSD
+				-	XfrCOC (Rev 11/01/94)
  Additional comments or instructions:
                                                                         26

-------
                                                                 PAGE 1  OP 1
                       TRIANGLE LABORATORIES, INC.
                      Transfer Chain-of -Custody Form
                              Project 43085
  Transfer  From:  DWLH5
                                              To:  DMS5
Initials..
                       Date
                                                        Time...
            Released  by:

            Accepted  by:
         MILES.ID,

         43085-
         43085-
         43085-
         43085-
         43085-
         43085-
         43085-
         43085-
         43085-
         43085-
         43085-
-000
-001
-002
-003
-004
-005
-006
-007
-008
-009
-010
         TLI NO	  Cust. Id,
TLI
181-
181-
181-
181-
181-
181
181
181
TLI
TLI
Blank
-55-1ABE
-55-2ABE
-55-3ABE
-55-4ABD
-55-5ABD
-55-6ABD
-55-7ABD
-55-8ABDE
LCS
LCSD
TLI M23 Blank
0-M23-1
O-M23-2
0-M23-3
0-M23-FB
I-M23-1
I-M23-2
I-M23-3
M23-RB
TLI LCS
TLI LCSD
Additional comments or instructions:
                                                      -XfrCOC  (Rev 11/01/94) —
                                                                        27

-------
                                                                                                                   PAGE 1 OF 1
I
|    Method:  Method 23:Tetra-Octa (Tol Combined)
|    Required Detection Limit: 0.05 ng
TRIANGLE LABORATORIES.  INC.
   HR GC/HRMS ANALYSIS
                                                            (PROJECT:    4308S
I
    SAMPLE INFORMATION
                                       1ST COLUMN
                                                                               2ND COLUMN
                                                            RS Cone
                                                       20 ill 9   100.0
I       I     TLI      /                | GC/MS FILENAME  (CONFIRM  (CONFIRM El LENAME^ I USF-RS      (USF-RS    (ANALYSIS
|S#.crd|  SAMPLE ID  /    CLIENT       (.COLUMN: 0^)5   |         I COLUMN: {/D dloO  (VOLUME      (INIT.     (COMMENTS
       |            /    SAMPLE ID     |                 |         |                   ISOLN ID     (DATE      |
                                                                                                            Spike File:  SPX23704

                                                                                                            Amt  cf  Extract:  ««0%
                                                                                                            --REV 03/07/95 (PSTMF

-------
                                                                 Kim uuy
        Instrument ID
         Column Type
                    Column ID
                               Plot Name
                                       Ini. Vol.
                                              Acquisition
                                                                                             Signature
                                                           G/C
                                                                                                         Date
      Filename
 Date
Time
Project #
Sample*
No.
Client Sample ID
Syr
332
                                                                                          "rr
Operalor/Oala
Comments'
                                                             7V/
                                                                                            V
                         /73'i
               V
                                   727
                                                                                                       m
                                                            TI-.
                                          TM
                                                       D
                                                            ILL
                        tLLL
                                             tA-lAC
                                                       Z
                                                                                          b 4
\/
                                                      J
                 \
                  L

                                                         \v
                                                                           r/W(/rms/hrrunlog doc (02/05/97)
    CO
                                        ConCal Due:
                                        ConCalDue:
                                                                                                             94
                                                                                                                   Page:

-------
•*
r J i"j \        |        '  ''     •
Transcribed from chromatographic data
Dated initials required
MvMAjafloons'hrrunlog.doc (02/05/97)
      /••*
              \^0^-
ConCal Due: _ /   •"
ConCal Due:	
                                                                                                                          Pane*

-------
                                                                     Run Log
Instrument ID Column Type Column ID

Plot Name Ini. Vol. Acquisition
T&JL 2-£/ ff>U/$-L.
?^z-??z^
Signature
G/C
?>/?Xf^
Date
*      Transcribed from chromatographic data
**      Dated initials required

sfvr1/qa/forms/hrrunlog doc (02/05/97)
 CO
ConCal Due:
ConCal Due:
It'.*2-
                                                        9G
                                                                                                                          Page:

-------
                                                             Triangle Laboratories, Inc.
                                                                    Run Log
Instrument ID Column Type Column ID Plot Name

Inj. Vol. Acquisition
cJhjLxQ EPMS 2.
/(ail. /^Kx^^-H^t
' Signature f^~
Q/C
'*///,-
'Date
*      Transcribed from chromatographic data
•*      Dated initials required

•rvr1/qa/forms/hrrunk)fl doc (02/05/97)
  CO .
ConCalDue:
ConCalDue:
5'-c/z.
                                                                                                                                   97

-------
                                                              •ftgfe Laboratories, inc.
                                                                   Run Log
        Instalment ID
Column Type
Column ID
Plot Name
 Ini. Vol.

O.o ^
Acquisition
                                                                                               Signature
G/C
                                                                                                  Date
*      Transcribed from chromatographic data
**      Dated initials required

srvrl/qg/dyms/hrruntog doc (02/05/97)
                               ConCalDue:
                               ConCalDue:
                                                                                                                      Dano*
                                                                                                                                99

-------
                                                       Triangle Laboratories, Inc.
                                                               Run Log
Instrument ID Column Tvpe Column ID Plot Name
^»0 p DPI tW G££0*ni Tt-f

Ini. Vol. Acquisition QIC
u^ l/aft*
Signature Date
Transcribed from chromatographic data
Dated initials required
              (02/05/97)
ConCal Due:
ConCal Due:

-------
                                                                   Run Log
Instrument ID Column Type Column ID
"•? 0 ? ^ & 7 1 *" £} k- £ 4 1 "!>

Plot Name !' Inj. Vol. Acquisition
' — ^s
1 M'vA L< — .
1 Signature
G/C
\)&T. L \"
W,,/i-v
Date
       Filename
Dale'
                        Time*
                 Project #
Sample*
No.
Client Sample ID
Syr
332
Operator/Date
                                                                                                                     Comments*
        t s'
3AiM.
                                                                         i.i
                                                                         ft*
                                                                                                ML
Kl
                    1.
                  I
                                                      T,
                                                                                     1,
                                     _iL
                                                                                             \ 3
                  s
i
                    I
                  ^
                     /
    yn^ Vu '!>
  *      Transcribed from chromatographic data
  **     Dated initials required

  srvr1/qa/forms/hrrunlog doc (02/05/97)
CO
Ul
                                        ConCal Due:
                                        ConCal Due:
                                                                                                                      Page:
                                                                                                              81

-------
SAMPLE
  DATA
           Triangle Laboratories, Inc.
   801 Capitola Drive        P.O. Box 13485
   Durham, NC 27713-4411      Research Triangle Park, NC
   919-544-5729           Fax * 919-544-5491

-------
                      TRIANGLE  LABORATORIES OF RTP,  INC.               Page  1
                   Sample  Result  Summary for Project 43085            09/18/97
                   Method  8290X Full  Screen Analyses (DB-5)
Data File             S975815           S975866          S975867          S975868
Sample ID        TLI  M23  Blank       O-M23-1          0-M23-2          0-M23-3

Units                   ng               ng               ng                ng
Extraction Date      09/04/97          09/04/97         09/04/97         09/04/97
Analysis Date        09/11/97          09/13/97         09/13/97         09/13/97
Instrument               S                S                S                 S
Matrix                  XAD           M23Train         M23Train         M23Train
Extraction Type       Soxhlet           Soxhlet          Soxhlet          Soxhlet
Analytes
2378-TCDD             (0.005)           (0.09)            (0.07)            (0.01)
12378-PeCDD           (0.006)           (0.1)              (0.09)            (0.01)
123478-HxCDD          (0.006)           (0.1)              (0.1)             (0.02)
123678-HxCDD          (0.005)           (0.1)              (0.1)             (0.02)
123789-HxCDD          (0.005.)           (0.1)              (0.1)             (0.02)
1234678-HpCDD         0.02            (0.2)              (0.2)             (0.03)
OCDD                   0.05            (0.5)              (0.6)             (0.10)
2378-TCDF              0.006           (0.08)            (0.05)            (0.006)
12378-PeCDF           (0.004)           (0.09)            {0.24}  E         (0.01)
23478-PeCDF           (0.004)           (0.09)            (0.07)            (0.01)
123478-HxCDF          (0.005)           (0.09)            (0.09)            (0.01)
123678-HxCDF          (0.003)           (0.07)            (0.07)            (0.01)
234678-HxCDF          (0.004)           (0.09)            (0.08)            (0.01)
123789-HxCDF          (0.005)           (0.1)              {0.24}  Q,E       (0.01)
1234678-HpCDF         0.02            (0.1)              (0.2)             (0.02)
1234789-HpCDF        (0.007)           (0.2)              (0.2)             (0.03)
OCDF                   0.03            (0.4)              (0.4)             (0.07)
TOTAL TCDD           (0.005)           (0.09)            (0.07)            (0.01)
TOTAL PeCDD           (0.006)           {0.53}            {1.0}             (0.01)
TOTAL HxCDD           (0.006)           (0.1)               0.44             (0.02)
TOTAL HpCDD            0.02            (0.2)              {1.0}             (0.03)
TOTAL TCDF            0.006             0.15             (0.05)            (0.006)
TOTAL PeCDF           (0.004)           (0.09)            {0.41}  E         {0.02}
TOTAL HxCDF           (0.004)           (0.09)            {0.46}E         (0.01)
TOTAL HpCDF            0.02            (0.2)             {0.36}            (0.02)

Other Standards Percent Recovery Summary  (%  Rec)
37C1-TCDD            94.6             79.3             100              101
 13C12-PeCDF  234     101     Q         71.8              93.1             93.4
 13C12-HXCDF  478      87.3             73.8              94.3   Q         85.0
 13C12-HXCDD  478      81.6             64.4    V         85.6   Q         83.2
 13C12-HpCDF  789      78.6             78.7             116     Q         86.7

Other Standards Percent Recovery Summary  (% Rec)
 13C12-HxCDF  789      69.4             74.3    Q         58.2   Q         84.8
 13C12-HxCDF 234      73.3             92.3              73.7   Q         94.6

 Internal Standards Percent Recovery Summary (% Rec)
 13C12-2378-TCDF     105     Q         137                88.1            114
 13C12-2378-TCDD      74.6             145                90.2             95.4
 13C12-PeCDF 123      94.4   Q         160      RO        82.1   Q,RO      91.9
 13C12-PeCDD 123     101     Q         177               102              100
 13C12-HxCDF 678      73.5             124                81.0   Q        103
 13C12-HxCDD 678      83.2             122                77.6   Q         92  2
 13C12-HpCDF 678      64.0              91.2              47.2   Q         64  7
 13C12-HpCDD 678      71.5              88.5              53.2   Q         63.8
 13C12-OCDD           73.1              60.5              29.8   Q         31.6
Triangle Laboratories, Inc.® Analytical Services Division
801 Capitola Drive • Durham, North Carolina 27713                                   Printed-16-26 09/1
Phone: (919) 544-5729 • Fax: (919) 544-5491

-------
                      TRIANGLE LABORATORIES  OF RTF,  INC.
                   Sample Result Summary  for Project 43085
                   Method 8290X Full  Screen  Analyses (DB-5)
                                                    Page 2
                                                   09/18/97

Data File
Sample ID

Units
Extraction Date
Analysis Date
Instrument
Matrix
Extraction Type

Analytes
2378-TCDD
12378-PeCDD
123478-HxCDD
123678-HxCDD
123789-HxCDD
1234678-HpCDD
OCDD
2378-TCDF
12378-PeCDF
23478-PeCDF
123478-HxCDF
123678-HxCDF
234678-HxCDF
123789-HxCDF
1234678-HpCDF
1234789-HpCDF
OCDF
TOTAL TCDD
TOTAL PeCDD
TOTAL HxCDD
TOTAL HpCDD
TOTAL TCDF
TOTAL PeCDF
TOTAL HxCDF
TOTAL HpCDF
 S975833
 0-M23-FB

   ng
09/04/97
09/11/97
    S
M23Train
 Soxhlet
                 S975834
                 I-M23-1

                   ng
                09/04/97
                09/11/97
                    S
                M23Train
                 Soxhlet
                 S975835
                 I-M23-2

                   ng
                09/04/97
                09/11/97
                    S
                M23Train
                 Soxhlet
                 S975843
                 I-M23-3

                   ng
                09/04/97
                09/11/97
                    S
                M23Train
                 Soxhlet
        B
        B
        B
{0.009}
 0.04
 0.02  Q
 0.03
 0.03
 0.03
 0.09
 0.02
 0.04
 0.04
 O.Q3
 0.03
 0.03
 0.03
{0.03} B
 0.02
 0.03
{0.009}
 0 .04
 0.09
 0.04
 0.02
 0.08
 0.11
 0.02
         B
(0.06)
(0.2)
(0.2)
(0.2)
(0.2)
(0.3)
 9.7
(0.05)
(0.09)
(0.09)
(0.1)
(0.1)
(0.1)
(0.2)
(0.2)
(0.2)
(0.3)
(0.06)
(0.2)
(0.2)
{0.35}
{0.18}
 0.47
(0.1)
(0.2)
 Other Standards Percent Recovery Summary (%  Rec)
 37C1-TCDD             95.6             102
 13C12-PeCDF 234       89.4
 13C12-HXCDF 478       83.1
 13C12-HxCDD 478       72.6    Q
 13C12-HpCDF 789       67.8    V
                  102
                   92.1
                  117
                   89.9
                  110
                         Q
                         Q
                         Q
 Other Standards Percent  Recovery Summary (% Rec)
 13C12-HXCDF 789       69.7              80.6   Q
 13012-HxCDF 234       81.5              76.4   Q

 Internal Standards  Percent Recovery Summary (% Rec)
 13C12-2378-TCDF       75.7
 13C12-2378-TCDD       71.5
 13012-PeCDF  123       75.4
 13C12-PeCDD  123       86.9
 13C12-HxCDF  678       81.3
 13C12-HXCDD  678       76.5
 13C12-HpCDF  678       75.9
 13C12-HpCDD  678       87.9
 13C12-OCDD            87.6
                    72.8
                      .3
                      .6
                  73.
                  50
                  45.4
                  65.4
                  70.9
                  56.0
                  59.6
                  55.8
                           Q
                           Q
                           Q
                           Q
                           Q
                           Q
(0.03)
(0.06)
(0.1)
(0.09)
(0.09)
(0.2)
 8.2
(0.02)
(0.04)
(0.04)
(0.06)
(0.05)
(0.06)
(0.07)
(0.1)
(0.1)
(0.4)
(0.03)
(0.06)
(0.10)
(0.2)
 0.17
 0.33
(0.06)
{0.26}
                 102
                  87.4
                 100
                  90.2
                  84.3
                                     49.8
                                     53.8
45.4
50.6
36.1
35.5
56.9
49.5
32.2
30.0
17.5


V,Q
V,Q




N
B
B
(0.005)
(0.009)
(0.01)
(0.01)
(0.01)
 0.14
16.2
 0.01
(0.005)
(0.005)
 0.02
(0.006)
{0.006}
(0.008)
 0.04  B
(0.02)
(0.05)
(0.005)
(0.009)
 0.02
 0.34
 0.01
{0.01}
 0.03
 0.04
                 103
                  93.4
                 112
                  99.8
                  75.7
                                                     54.2
                                                     73.5
                                    63.3
                                    58.5
                                    56.9
                                    57.2
                                    64.5
                                    58.0
                                    35.3
                                    29.8
                                    16.0
                         V
Triangle Laboratories, Inc.® Analytical Services Division
801 Caprtola Drive • Durham, North Carolina 27713
Phone: (919) 544-5729 • Fax: (919) 544-5491
                                                      Printed: 16:26

-------
TRIANGLE LABORATORIES OF RTF, INC. Page 3
Sample Result Summary for Project 43085 09/18/97

Data File
Sample ID
Units
Extraction Date
Analysis Dace
Instrument
Matrix
Extraction Type
Analytes
2378-TCDD
12378-PeCDD
123478-HxCDD
123678-HxCDD
123789-HxCDD
1234678-HpCDD
OCDD
2378-TCDF
12378-PeCDF
23478-PeCDF
123478-HxCDF
123678-HxCDF
234678-HxCDF
123789-HxCDF
1234678-HpCDF
1234789-HpCDF
OCDF
TOTAL TCDD
TOTAL PeCDD
TOTAL HxCDD
TOTAL HpCDD
TOTAL TCDF
TOTAL PeCDF
TOTAL HxCDF
TOTAL HpCDF
Method 82 9 OX
S975844
M23-RB
ng
09/04/97
09/11/97
S
M2 3 Train
Soxhlet

(0.004)
(0.005)
(0.005)
0.006
0.007
0.03 B
0.05 B
(0.003)
(0.004)
{0.005}
0.03
0.01
0.01
(0.003)
0.05 B
{0.008}
0.05 B
{0.007}
{0.01}
0.01
0.04
(0.003)
0.007
0.07
0.07
Full Screen Analyses (DB-5)
S975831
TLI LCS
ng
09/04/97
09/11/97
S
XAD
Soxhlet

0.36
1.8
1.8
1.8
1.8
1.7
3.4
0.36
2.0
1.8
1.7
1.7
1.6
1.5
2.1
1.5
2.7








S975832
TLI LCSD
ng
09/04/97
09/11/97
S
XAD
Soxhlet

0.36
1.9
1.7
1.8
1.9
1.8
3.6
0.37
1.9
1.9
1.7
1.8
1.7
1.8
1.8
1.6
2.8








 Other Standards Percent Recovery  Summary (% Rec)
 37C1-TCDD           105
 13C12-PeCDF 234      95.0
 13C12-HxCDF 478      89.0
 13C12-HxCDD 478      87.7
 13C12-HpCDF 789      97.8

 Other Standards Percent Recovery  Summary (% Rec)
 13C12-HxCDF 789      75.8              72.3             75.4
 13C12-HxCDF 234      79.3              76.2             77.5

 Internal Standards  Percent Recovery Summary  (% Rec)
 13C12-2378-TCDF      68.5
 13C12-2378-TCDD      61.5
 13C12-PeCDF 123      67.5
 13C12-PeCDD 123      69.2
 13C12-HxCDF 678      75.6
 13C12-HXCDD 678  .    69.2
 13C12-HpCDF 678      60.9
 13C12-HpCDD 678      66.8
 13C12-OCDD           60.2

 {Estimated Maximum Possible Concentration},   (Detection  Limit)
64.9
62.6
65.3
69.4
72.8
73.1
58.4
64.5
56.7
65.4
60.9
64.9
66.7
72.8
70.3
62.5
67.1
60.2
Triangle Laboratories, Inc.® Analytical Services Division
801 Capitola Drive • Durham, North Carolina 27713
Phone: (919) 544-5729 • Fax: (919) 544-5491
Printed: 16:26

-------
                       TRIANGLE LABORATORIES OF RTP,  INC.
                    Sample Result Summary for Project 43085
                              Method  23X (DB-225)
                                                         Page  1
                                                        09/18/97
Data File
Sample  ID

Units
Extraction Date
Analysis Date
Instrument
Matrix
Extraction Type

Analytes
2378-TCDF
    P973852
TLI M23 Blank
P973854
I-M23-3
P973861
0-M23-FB
ng
09/04/97
09/12/97
P
XAD
Soxhlet
ng
09/04/97
09/12/97
P
M23Train
Soxhlet
ng
09/04/97
09/13/97
P
M23Train
Soxhlet
     (0.03)
 (0.03)
 Internal Standards Percent Recovery Summary  (% Rec)
 13C12-2378-TCDF      67.4              53.9
 (0.05)
                                         70.9
 (Detection Limit).
Triangle Laboratories, Inc.® Analytical Services Division
801 Caprtola Drive • Durham, North Carolina 27713
Phone: (919) 544-5729 • Fax: (919) 544-5491
                                                            Printed: 16:14 09/1 j

-------
                                     TRIANGLE LABORATORIES.  INC.
                          LAB CONTROL SPIKE RECOVERY  ANALYSIS AND COMPARISON

                                            Project:  43085
                                             Matrix:  XAD
                                         Method:  Modified 23

ID:
I some r

!378-TCOD
2378-PeCDD
123478-HxCDO
123678-HxCDD
123789-HxCOO
1234678-HpCDO 0
5CDD 0
2378-TCDF 0
12378-PeCOF
23478-PeCDF
123478-HxCDF
23678-HxCDF
234678-HxCDF
123789-HxCOF
1234678-HpCDF 0
1234789-HpCOF
DCDF 0
SO: Not Detected
4A: Not Applicable
[..]: EMPC Value

S975815
TLI M23 Blank
Samp le
(ng)
ND
NO
NO
ND
ND
.02
.05
.006
NO
ND
ND
ND
NO
ND
.02
ND
.03



Processed By:
S975831
ID: TLI LCS
With Spike
(ng)
0.36
1.8
1.8
1 .8
1.8
1.7
3.4
0.36
2.0
1 .8
1 .7
1.7
1.6
1 .5
2.1
1 .5
2.7



.3L-/«.,
S975832

Percent
Recovery
89.5
91.7
87.5
89.1
89.4
84.5
84.9
88.6
101
91.1
85.3
84.2
80.0
76.7
102
77.2
68.0



•tj
ID: TLI
Spike
(ng)
0.36
1.9
1.7
1.8
1.9
1.8
3.6
0.37
1.9
1.9
1 .7
1.8
1.7
1.8
1 .8
1.6
2.8



Date:
LCSD
Dup Percent
Recovery
89.1
93.6
87.4
. 90.4
94.9
87.7
88.7
89.9
94.7
95.0
86.3
87.8
83.5
90.4
90.6
80.6
70.2



09/18/97
Relative
Percent
Difference
0.45
2.05
0.11
1.45
5.97
3.72
4.38
1.46
6.44
4.19
1.74
4.19
4.28
16.4
11 .8
4.31
3.18
MILES 4.15.00
GRY_PSUM v1 .01


ercent  Recovery  QC  Limits: 70 to 130 percent.
elative Percent  Difference QC Limits: +/-  20 percent.

ote:  Method 23 does not  address spiked samples.   Triangle Labs
     uses Method 8290  control  limits as advisory  guidelines.

ominal  Spike Levels (ng):
    TCDD/TCDF..:  0.4 ng
    PeCDD/PeCOF:  2.0 ng
    HxCDO/HxCDF:  2.0 ng
    HpCDD/HpCOF:  2.0 ng
    OCDD/OCDF..:  4.0 ng
                                                                                                                        41

-------
TLI Project:     43085
Client Sample:   TLI M23 Blank
Method 23 PCDD/PCDF Analysis (a)
            Analysis File:   S975815
Client Project:
Sample Matrix:
TLI ID:

Sample Size:
Dry Weight:
GC Column:
S413-004
XAD
TLI Blank

1.000
n/a
DB-5

Date Received:
Date Extracted:
Date Analyzed:
Dilution Factor:
Blank File:
Analyst:

II
09/04/97
09/11/97
n/a
S975815
HLM

Spike File:
ICal:
ConCal:
% Moisture:
% Lipid:
% Solids:

SPX23704
SF56117
S975814
n/a
n/a
n/a
to&ytes^ ,-^m^
2,3,7,8-TCDD
1,2,3,7,8-PeCDD
1,2,3,4,7,8-HxCDD
1,2,3,6,7,8-HxCDD
1,2,3,7,8,9-HxCDD
1,2,3,4,6,7,8-HpCDD
1,2,3,4,6,7,8,9-OCDD
2,3,7,8-TCDF
1,2,3,7,8-PeCDF
2,3,4,7,8-PeCDF
1,2,3,4,7,8-HxCDF
1,2,3,6,7,8-HxCDF
2,3,4,6,7,8-HxCDF
1,2,3,7,8,9-HxCDF
1,2,3,4,6,7,8-HpCDF
1,2,3,4,7,8,9-HpCDF
1,2,3,4,6,7,8,9-OCDF
S*^ ">*'-•
Total TCDD
Total PeCDD
Total HxCDD
Total HpCDD
Total TCDF
Total PeCDF
Total HxCDF
Total HpCDF
%*$fttat (ng>
ND
ND
ND
ND
ND
0.02
0.05
0.006
ND
ND
ND
ND
ND
ND
0.02
ND
0.03
Amt (ng)
ND
ND
ND
0.02
0.006
ND
ND
0.02
DL EMPC
0.005
0.006
0.006
0.005
0.005



0.004
0.004
0.005
0.003
0.004
0.005

0.007

Number DL EMPC
0.005
0.006
0.006
1
1
0.004
0.004
1
fiaifo fit £tegs





1.07 32:01 ~~
0.84 34:33 	
0.85 20:25 	






1.18 31:11

0.76 34:39
Flags



—




                                       Page 1 of 2
                          X237 J>SR V2.00. LARS «.U
 Triangle Laboratories, Inc.®
 801 Capitola Drive • Durham, North Carolina 27713
 Phone: (919) 544-5729 • Fax: (919) 544-5491
                       Printed 13:58
0942

-------
TLI Project:      43085
Client Sample:   TLI M23 Blank
Method 23 PCDD/PCDF Analysis (a)
             Analysis File:  S975815
trtternarstandards
13C12-2,3,7,8-TCDF
13C.2-2,3,7,8-TCDD
13C,2-l,2,3,7,8-PeCDF
13C,2-l,2,3,7,8-PeCDD
13C12-l,2,3,6,7,8-HxCDF
13C,2-l,2,3,6,7,8-HxCDD
13C,2-l,2,3,4,6,7,8-HpCDF
13C,2-l,2,3,4,6,7,8-HpCDD
13CP-1,2,3,4,6,7,8,9-OCDD

Surrogate Standards (Type A)
37CL,-2,3,7,8-TCDD
13C,2-2,3,4,7,8-PeCDF
13C,2-l,2,3,4,7,8-HxCDF
13Ci2-l,2,3,4J.8-HxCDD
13Ci2-l,2,3,4,7,8,9-HpCDF

Alternate Standards (Type A)
13C,2-l,2,3,7,8,9-HxCDF
13C12-2,3,4,6,7,8-HxCDF
Recovery Standards
13C12-1,2,3,4-TCDD
13C12-l,2,3,7,8,9-HxCDD
Amt (ng)
4.2
3.0
3.8
4.1
29
3.3
2.6
2.9
5 8

AmL (ng)
3.8
4.0
3.5
3 3
3 i

Amt (ng) :;
2.8
2.9


% Recovery
105
74.6
94.4
101
73 5
83.2
64.0
71.5
77 i

% Recovery;
94.6
101
87.3
91 f.
78 f\

|J:pi Recovery
69.4
73.3


QC Limits
40%- 130%
40%- 130%
40%- 130%
40%-130%
/inoji.i^n^
40%- 130%
25%- 130%
25%- 130%

QC Limits
70%- 140%
70%- 140%
70%-1407o
~IC\OJ. \Af\C!..
~I(\O!- 1 /tnor.

; QC Limits
40%- 130%
40%- 130%


Ratio
0.76
0.80
1.70
1.41
0 J.Q
1.18
0.43
0.95
078
. /o
Ratio
1.51
0.51
11 C
.13
OA1
.**3
: Ratio ?
0.48
0.50
Ratio
0.81
i m
RT
20:23
21:13
24:42
25:50
29:11
31:11
32:02

RT
21:13
25:28
28:22

oL.2.5
^.•:.RT::.:.,
29:41
28:59
RT
21:00
Flags
Q_
OH
Q_
—

«*8ts.
oil
	
~
Ffafs
—
Flags !
—~~.
                     Data Reviewer
Triangle Laboratories, Inc.®
801 Capitola Drive • Durham, North Carolina 27713
Phone: (919) 544-5729 • Fax: (919) 544-5491
                                                           09/17/97
                                       Page 2 of 2
                                                                         X237 J>SR vZOO. LARS 6 1O.O4
                      Printed: 13:58 09/1

-------
Data Review By:
Initial    ....Date...

  *tf\~/    5_/J3L/2i:  Calculated Noise Area:
                                                                      1.55
The Total Area for each peak with an ion abundance ratio outside
ratio limits has  been  recalculated according  to  method requirements.
Page No.
09/17/97
 Listing of S975815B.dbf
 Hatched GC Peaks  /  Ratio  / Ret. Time
Compound/
M_2.... QC.Log Omit Why
TCDF
304-306
        D

        M


 304-306

 13C12-TCDF
 316-318
  .RT. OK Ratio Total.Area... Area.Peak.1..  Area.Peak.2..  Rel.RT Compound.Name.. ID.. Flags.
 316-318

DC
DC
DC
DC
DC

DC
DC


DC
DC






NL
SN
SN
SN
SN

SN
SN
1

NL
WL




4

0:
17:
19:
19:
20:
20:
20:
22:

00
38
40
57
14
25
58
;17
0.
RO
RO
RO
RO


RO
RO
65-0.89
0.
0.
2.
0.
0.
0.
1.
0.
10
93
17
56
76
35
39
35
Peak

0
19
19
19
20
20

:00
:11
:32
:54
-.23
:51
0.
RO

RO
RO

RO
0.
1.
1.
6.
1.
8.
2.
4.
8.
18
61
93
21
94
52
62
07
52
65-0.89
0
0
0
0
0
1
.55
.69
.57
.59
.76
.23
Peaks
1.
49
6
25
4,593
19
4,645
.56
.17
.64
.77
.60
.88
.89
0.820-1.101
0.
0.
0.
0.
0.
3.91 4.61 1.
1.
1.

000
865
965
979
993
002 2378-TCDF AN
029
093

0.951-1.049
0
0
2.89 5.03 0
11.21 18.88 0
1,979.96 2,613.64 1
13.84 11.23 1

.000
.941
.958
.976
.000 13C12-2378-TCDF ISO
.023

                                       Above:  TCDF / TCDD Follows
 TCDD
 320-322
  320-322
0.65-0.89
DC
DC
DC
DC
DC
DC
DC
DC
DC
DC
DC
DC
DC
DC
DC

NL
SN
SN
SN
SN
SN
SN
SN
SN
SN
SN
SN
SN
SN
WH
0
0:
18:
18:
20:
00
15
42
:01
20:23
20
20
20
21
21
21
21
22
22
22
:37
:38
:58
:13
:28
:40
:42
:01
:15
:37
RO
RO
RO
RO
RO
RO
RO
RO
RO
RO
RO
RO
RO
RO
RO
5.
4.
3.
0.
4.
1.
6.
2.
0.
0
1
0
4
0
5
13
53
00
44
40
43
69
.84
.30
.29
.86
.18
.69
.94
.70
Peaks
                                                0.14
                                                0.30
                                                0.30
                                                1.52
                                                1.20
                                                0.25
                                                0.28
                                                0.78
                                                2.09
                                                0.87
                                                0.25
                                                0.16
                                                0.62
                                                1.38
                                                0.41
                                                0.00
                                                      0.853-1.059
                                                          0.000
                                                          0.860
                                                           .381
                                                           .943
                                 0.
                                 0.
                                 0.961
                                 0.972
                                 0.973
                                 0.988
                                 1.000 2378-TCDD
                                 1.012
                                 1.021
                                 1.023
                                 1.038
                                 1.049
                                 1.066
                                                                               AN
  37C1-TCDD
  328
                  DC
                  DC
                     NL
   0:00
   0:00
  19:40
 0.08
 0.00
13.92
                                                             13.92
0.906-1.094
    0.000
    0.000
    0.927
 Triangle Laboratories, Inc.® Analytical Services Division
 801 Capitola Drive • Durham, North Carolina 27713
 Phone: (919) 544-5729 • Fax: (919) 544-5491
                                                                        Printed: 1359 09/17/9'
                                                                                                              44

-------
Page No.     2
09/17/97


Compound/
M_Z.... QC.Log Omit Why
Listing  of S975815B.dbf
Hatched  GC Peaks / Ratio  / R«t. Time
.RT.  OK Ratio Total.Area... Area.Peak.1.. Area.Peak.2..  Rel.RT Compound.Name..  ID.. Flags.
AM
328
13C12-TCDD
332-334








332-334
PeCDF
340-342













340-342
13C12-PeCDF
352-354







352-354
DC

DC
DC
DC

DC



DC


DC
DC
DC
DC
DC
DC
DC
DC
DC
DC
DC
DC
DC
DC


DC








SN :
5

NL
WL
SN

SN



SN
4

NL
SN
SN
SN
SN
SN
SN
SN
SN
SN
SN
SN
SN
WH
0

NL







7
21:13
21:29
21:38
21:42
22:01
Peaks
O.i
0:00 RO :
19:05 RO
19:29 RO
19:54 RO
20:36
21:00
21:13
21:34 RO
22:00 RO
Peaks
1.
0:00 RO
22:56 RO
23:04 RO
23:31 RO
23:50 RO
24:10 RO
24:27 RO
24:35 RO
24:45 RO
25-. 16 RO
25:48 RO
26:28 RO
26:36 RO
26:43 RO
Peaks
1
0:00 RO
23:49
24:20
24:42
25:00
25:28
25:50 RO
26:27 RO
Peaks
2,:
2,:
55-0.89
20.25
0.91
1.16
1.05
0.84
0.81 3,
0.80 2,
1.08
0.35
6,
32-1.78
0.09
0.09
0.52
0.30
0.61
0.27
2.73
2.15
0.79
0.50
1.13
0.23
0.31
0.78

.32-1.78
1.00
1.62
1.60
1.70 3
1.58
1.51 3
1.93
1.23
7
L10.00 2,110.00
2.91 2.91
2.91 2.91
2.17 2.17
1.01
131.91

0.14
2.46
1.31
16.35 9.69
3.83
329.10 1.490.55
645.89 1,177.55
41.54 25.41
1.54
032.88
TVT\n / DttfTMT V rtl 1 *-\ue
l\~UU f few IJJT rOll OWS - " '
0.12
0.10
0.54
0.59
2.88
1.07
4.74
0.84
2.68
2.02
0.15
0.81
0.64
2.20
0.00

0.15
56.50 34.94
20.27 12.47
,558.95 2,241.95
33.92 20.75
,479.61 2,092.50
6.17 4.68
10.18 6.19
,165.60
1.000 37C1-TCDD :
1.013
1.020
1.023
1.038
0.906-1.094
0.000
0.899
0.918
9.24 0.938
0.971
1,838.55 0.990 13C12-1234-TCDD
1,468.34 1.000 13C12-2378-TCDD
23.47 1.016
1.037

0.907-1.078
0.000
0.928
0.934
0.952
0.965
0.978
0.990
0.995
1.002 12378-PeCDF
1.023
1.045
1.072
1.077
1.082

•0.838-1.162
0.000
21.56 0.964
7.80 0.985
1,317.00 1.000 13C12-PeCDF 123
13.17 1.012
1,387.11 1.031 13C12-P6CDF 234
2.42 1.046
5.04 1.071

SOR1






RSI
IS1












AN










IS2

SUR2



                                     Above:  PeCDF / PeCDD Follows
Triangle Laboratories, Inc.® Analytical Services Division
801 Capitola Drive • Durham, North Carolina 27713
Phone: (919) 544-5729 • Fax: (919) 544-5491
                                                                     Printed: 13:59 09/17/
ft

-------
Page No.
09/17/97
Listing of S975815B.dbf
Hatched GC Peaks / Ratio / Ret.
Tin
Compound/
M_Z....  QC.Log Omit Why  ..RT. OK Ratio Total.Area... Area.Peak.1.. Area.Peak.2..  Rel.RT CoBpound.Name.. ID.. Flags.
PeCDD
356-358



D


356-358
13C12-PeCDD
368-370







368-370

HXCDF
374-376


D



D


D
374-376
13C12-HXCDF
384-386













1.32-1.78
DC NL 0: 00 RO 12.71
DC SN 23:59 1.63
DC SN 24:43 RO 7.49
DC SN 25:00 RO 0.53
DC SN 25:51 RO 1.18
DC SN 26:19 RO 0.77
DC SN 26:30 RO 4.30
0 Peaks
1.32-1.78
DC NL 0:00 RO 1.00
DC SN 24:01 RO 0.86
DC SN 24:42 1.71
DC SN 24:52 RO 3.69
DC SN 25:34 RO 1.27
25:50 1.41
25:59 1.52
DC SN 26:34 RO 1.89
2 Peaks

1.05-1.43
DC NL 0:00 RO 1.91
DC SN 27:35 1.20
DC SN 28:17 RO 3.04
DC SN 28:23 1.05
DC SN 28:28 RO 0. 56
DC SN 28:43 RO 0.85
DC SN 28:53 RO 0.50
DC SN 28:59 RO 0.96
DC SN 29:06 RO 1.84
DC SN 29:22 RO 0.13
DC SN 29:37 1.19
0 Peaks
0.43-0.59
DC NL 0:00 RO 0. 91
27:21 RO 0.41
27:29 0.53
28:22 0.51
28:28 0.49
28:37 RO 0.62
28:59 0.50
29:08 0.46
DC SN 29:22 0.59
DC SN 29:27 RO 0.31
DC SN 29:33 RO 0.72
29:41 0.48
DC SN 29:55 RO 0.97
DC SN 30:11 RO 0.34

0.18
2.18
1.05
1.14
4.16
0.76
0.94
0.00

0.13
1.32
3.60
1.71
2.76
2,144.29 1,255.11
196.92 118.64
2.40
2,341.21


2.46
2.13
2.44
10.30
1.61
1.48
1.16
6.94
1.28
0.11
8.15
0.00

2.97
8.50 2.87
23.70 8.20
2.397.48 812.87
2,862.76 938.49
10.45 4.29
2,646.33 878.42
8.99 2.82
1.99
2.10
1.48
2,176.54 708.64
2.94
1.39
0.921-1.026
0.000
0.928
0.957
0.968
1.001 12378-PeCDD AN
1.019
1.026

0.845-1.155
0.000
0.930
0.956
0.963
0.990
889.18 1.000 13C12-PeCDD 123 IS3 Q
78.28 1.006
1.028


0.955-1.052
0.000
0.969
0.994
0.997 123478-HxCDF AN
1.000 123678-HXCDF AN
1.009
1.015
1.018 234678-HxCDF AN
1.022
1.032
1.040

0.859-1.141
0.000
7.04 0.961
15.50 0.965
1,584.61 0.996 13C12-HXCDF 478 SUR3
1,924.27 1.000 13C12-HXCDF 678 IS4
6.92 1.005
1,767.91 1.018 13C12-HXCDF 234 ALT2
6.17 1.023
1.032
1.035
1.038
1,467.90 1.043 13C12-HXCDF 789 ALT1
1.051
1.060
 Triangle Laboratories, Inc.® Analytical Services Division
 801 Capitola Drive • Durham, North Carolina 27713
 Phone: (919) 544-5729 • Fax: (919) 544-5491
                                                                     Printed 13:59 09/1^*

-------
Page No.
09/17/97
Listing of S975815B.dbf
Matched GC Peaks / Ratio
/ Ret. Time
Confound/
M_Z.... QC.Log Omit  Why  ..RT. OK Ratio Total.Area... Area.P»ak.l. . Area.Peak.2.. Rel.RT Compound.Name.. ID.. Flags.
384-386
                     8 Peaks
                                        10,134.75
HxCDD
390-392





D


390-392
13C12-HXCDD
402-404







402-404

HpCDF
408-410
MKT


D


408-410
13C12-HpCDF
418-420



418-420
HpCDD
424-426


1.05-1.43
DC
DC
DC
DC
DC
DC
DC
DC
DC


DC





DC
DC



DC

DC
DC
DC
DC
DC


DC

DC



DC
DC
DC
NL
SN
SN
SN
SN
SN
SN
SN
WH
0

NL





SN
SN
5


NL

SN
SN
SN
WH
WH
1

NL

SN

2

NL
SN
SN
0:00
28:21
28:28
28:54
29:12
29:19
29:24
29:28
29:48
Peaks

0:00
28:35
29:06
29:11
29:29
29:40
29:45
29:49
Peaks


0:00
31:11
31:33
32:10
32:24
32:39
32:53
Peak

0:00
31:11
31:26
32:23
Peaks

RO
RO .
RO
RO
RO
RO

RO
RO

1.

RO



RO
RO
RO
0.
3.
1.
2.
1.
0.
1.
2.
1.

80
97
49
55
95
41
33
91
56

1.
0.
2.
0.
1.
1.
5.
0.
0.
0.
75
72
SO
65
84
16
20
72
56
00
05-1.43
1.
0.
1.
1.
1.
1.
0.
1.
40
99
15
18
19
00
.73
.45
1.
25
12.77 7.07
2,128.76 1.138.54
2,679.88 1.451.98
3,236.46 1,760.90
6.79 3.76
1.70
2.22
0.950-1.015
0.
0.
0.
0.
1.
1.
1.
1.
1.

000
971
975
990
001 123678-HXCDD
005
007
010 123789-HxCDD
021





AN


AN


0.966-1.034
0.
7.15 0.
990.22 0.
1,227.90 1.
1,475.56 1.
3.75 1.
1.
000
979
997 13C12-HXCDD 478
000 13C12-HXCDD 678
010 13C12-HXCDD 789
017
019


SUR4
IS5
RS2


1.022
8,064.66

0.
RO


RO
RO
RO
RO

0
RO

RO



88-1.20
1
1
1
0
0
0
2

.37
1
0
1
0
-S3
.18
.09
.26
.87
.29
.24

-0.51
.34
.43
.87
.43
• Uv(—r^n / Urs/^TM? C"/N! 1 rtwe
nxuuLf / npcur follows —
0
14
3
0
5
0
1
14
.94
.68 7.95
.15
.45
.98
.31
.90
.68
0.995-1.044
0
6.73 1
1
1
1
1
1

.000
.000 1234678-HpCDF
.012
.032
.039 1234789-HpCDF
.047
.055


AN


AN



0.936-1.128
1
1,836
1
1,113
.18
.69 550.23
.90
.47 333.82
0
1,286.46 1
1
779.65 1
.000
.000 13C12-HpCDF 678
.008
.038 13C12-HpCDF 789

IS6

SUR5
2,950.16
0
0:00 RO
31:17 RO
31:28 RO
.88
7
1
3
-1.20
.14
.37
.09

tr i npv,uu TUJ.J.OWS --
0.14
1.20
1.41
0.976-1.006
0
0
.000
.977


0.982
Triangle Laboratories, Inc.® Analytical Services Division
801 Capitola Drive • Durham. North Carolina 27713
Phone: (919) 544-5729 • Fax: (919) 544-5491
                                                                    Printed: 13:59 09/

-------
Page No.
09/17/97
        Listing  of S975815B.db«
        Macchod  QC Peaks / Ratio / Ret. Tim*
Compound/
M_Z....  QC.Log omit Why  ..RT. OK Ratio Total.Area... Area.Peak.1..  Area.Peak.2..  Rel.RT Compound.Name..  ID.. Flags.
                DC   SN  31:39 RO  2.30
        MT              32:01     1.07
424-426               1  Peak
                              0.94
                              7.73
                              7.73
4.00
              3.73
     0.988
     0.999  1234678-HpCDD
                                          AN
13C12-HpCDD                    0.88-1.20
436-438         DC  NL   0:00      1.11          3.77
                        31:26  RO .  1.25          7.08
                        32:02      0.95       1,887.05
436-438               2 Peaks                1,894.13
                                            4.33
                                           918.59
                0.969-1.031
                    0.000
              3.47  0.981
            968.46  1.000 13C12-HpCDD 678 IS7
OCDF
442-444
 442-444
0.76-1.02
DC
DC
DC
DC
DC
DC
DC
DC
DC
DC
DC
DC

DC
DC
DC

NL
SN
SN
SN
SN
SN
SN
SN
SN
SN
SN
SN

SN
SN
SN
1
0:00
30:
31:
31:
31:
32:
32:
32;
33;
33;
33
34
34
35
35
35
55
21
41
58
19
32
41
09
:15
:33
:24
:39
:18
:40
:54
RO
RO
RO
RO

RO
RO
RO
RO
RO
RO

RO
RO
RO
0.
1.
1.
0.
0.
1.
2.
0.
2.
0.
0
0
0
1
0
0
89
16
14
04
08
00
93
.68
,28
.36
.67
.34
.76
.94
.15
.64
Peak
                                      Above:  HpCDD  / Octa-CDD and CDF Follows
                                                0.68
                                                1.61
                                                0.40
                                                0.13
                                                0.13
                                                0.66
                                                0.57
                                                1.06
                                                0.55
                                                0.51
                                                0.76
                                                1.32
                                               13.25
                                                0.93
                                                0.49
                                                0.64
                                               13.25
                                             5.71
                                                            0.884-1.116
                                                                0.000
                                                                0.895
                                                                  .908
                                                           7.54
                    0.
                    0.917
                    0.926
                    0.936
                    0.942
                    0.946
                    0.960
                    0.963
                    0.972
                    0.996
                    1.003 OCDF
                    1.022
                    1.033
                    1.040
                                                                                       AN
 OCDD
 458-460
 458-460
               0.76-1.02
DC  NL   0:00     1.00
        34:33     0.84
DC  SN  34:46 RO  3.00
      1 Peak
                                                0.14
                                               17.46
                                                0.30
                                               17.46
 7.98
  0.884-1.116
      0.000
9.48  1.000  OCDD
      1.007
                                           AN
 13C12-OCDD                     0.76-1.02
 470-472         DC  NL   0:00     1.00          0.14
                         34:32     0.78      2,454.20
 470-472               1 Peak                2,454.20
                                          1,074.52
                                                             0.995-1.005
                                                                 0.000
                                                        1,379.68  1.000 13C12-OCDD
                                                                                       1S8
 Column Description.
                 "Why" Code Description	   QC Log Desc.
 M_Z   -Nominal Ion Mass(es)
  . .RT. -Retention Time (mm:ss)
 Rat.l -Ratio of M/M+2 Ions
 OK
       -RO=Ratio outside Limits
  Rel.RT-Relative Retention Time
     End of Report
                                 WL-Below Retention Time Window  A-Peak Added
                WH-Above Retention Time Window
                SN-Below Signal to Noise Level
                
-------
rile>SS75815 #1-848 Acq:ll-SEP-1997 03:08,30 SI+ Voltage SIX 70S Noiu»t3B
303.9016 Tt2 BSUB<256,30,-3.0)  PKD(9,5,5,0.05\,152.0,1.00\,r,T) Exp:ETCUS
TRIANGLE LABS  Text:Til M23  BLANK  TLIH308S                IJKT. TIME -    03t09
                                                           A5.07E4
      17:00           18:00           19:00           20:00           21:00
r±le:S975815 #1-848 Acq:ll-SEP-1997 03:08:30 EH- Voltage SIS 70S O6ime:384
305.8987 Ts2 BSUB(256,30,-3.0)  PKD(9,5,5,0.05\,1536.0,1.00%,T,T) ExpiEfCOS
TRIANGLE LABS  Text!ITJ M23  BLANK  TLH43085                1ST. TIME  -   03:09
1003

  aol
                                                                                     22 tOO
      17:00           18:00           15.-00           20': 00           21:00
file:S975815  #1-848  Acqsll-SEP-1997 03:08:30 EI+ Voltage SIR  70S Noiae:342
315.9419 T:2  BSU3(256,30r -3.0) PKD(9,5,5, 0. 051,1368. 0,1. 00\,r,T) Exp:EPCUS
TRIANGLE LABS  Text:TLI M23 BLANK  TLI#43085                ISJ. TIME '   03:09
                                                                                     22:00
1003

  80.

  601

  40,
  201

   OJ
                                                           A1.98E7
                                                                                                     -4.7E6

                                                                                                     .3. 8E6

                                                                                                     .2.8E6

                                                                                                     .1. 9E6

                                                                                                     .9. 4E5
                                        T
                                                       "T
      -I7.-00           18:00           1P.-00           20:00
rile:S975815  #1-848 Acq:ll-SEP-1997 03:08:30 EI+ Voltage  SIR  70S Noiae:613
317.9389  F:2  BSUB(256,30, -3 .0} PKD(9, 5,5, 0. 05\,2452.0,1 . 00\,F,T) Exp:EPCUS
TRIANGLE  LABS  Text:TLI M23 BLANK  TLI443085                IKJ. TIME -   03:09
1003

  aol
  40.

  201

   ol
                                                                                     ""	1	""
                                                                                     22: 00
O.OEO
   Time
                        ~T
                                                        T
                                                                                                     -6.3E6

                                                                                                     .5. OE6

                                                                                                     .3.8E6

                                                                                                     .2.5E6

                                                                                                     '•.1.3X6
                                                                      21': 00
      17:00           18:00           19:00           20:00
F±le:S975815 #1-848 Acq:ll-SEP-1997 03:08:30 Eli- Voltage SIR 70S
330.9792 T:2 ExpiEPCUS
TRIANGLE LABS  Text:TLI M23 BLANK  TLH43085                1X7. TIME  -
                                                                                      22:00
O.OEO
   Tine
                                                                            03:09
                                                                      21:00
      17:00           18:00           19': 00           20:00
File:S975815  #1-848  Acq:ll-SEP-1997 03:08:30 EH- Voltage SIR  70S
375.8364 r:2  ExptEPCUS
TRIANGLE LABS  TextiTLI M23 BLANK  TLI#43085                UKT.  TIME -   03:09
1001
                                                                                      22:00
                                                                                                           48

-------
rile:S975815 #1-848 Acq: ll-SXP-1997 03:08:30 EH- Voltage SIX 70S Noim«:206
319.8965 r:2 BSUB(256, 30, -3 .0) PXD(7,5
,3, 0.05%, 82*.
TRIANGLE LABS Text:TLI M33 BLANK TLH43085
1001
80.
60:
40:
20.
o'\



A1.30E4
..JiJIljCiUui^L

Al.

il

AwMtl
20:00'
0,1.00\,F,T) XxptXPCOS
INJ. TIMX - 03:09
9X4 1.2X4


AS 94X3 '
rMs^M^^ \
9.5X3
7.1X3
4 7F1
v . / &J
2.4X3
n nrn
'21:00 	 22:00' ' Ti"«
rile:S975815 #1-848 Acq i ll-SXP-1997 03:08:30 XI* Voltage SIX 70S Noise: 40 , f £.f~X7-VJ{ .?<{}-,
321.8936 F:2 BSUB(256, 30, -3.0) PKD(7 , 5,3,0 .05\, 160
TRIA1
100J
80:

60:

40:

20:
o:
1GLE LABS Text: TL I M23 BLANK TLH43085
Al . 65X4


AS. 40X3

1 I 1
II A9.88J 3 S 1 »7 1g*1
|h i I Al A \ Hi A
JUiWiWiJV^ S\M JVl^'iA^''vA-M'^wvvj
19:00


A1.51E4
I

| \A6.17E3
\ II I h C KA
l/i All, » iikAl.
^VilNWINr
20:00'
0,1.00*,f,rj Exp:EPCUS V v £11-*'
INJ-. TIHX • 03s 09 Cjv'a"'"
A3.07E4 / 8.4X3

A7.79X3

A1.13E4 \kl.32E4 .



\M/J \/WvL/rA\r V VA/iyVr^V (vw I WrX'nVWp
.6.7X3

.5.0X3

.3 . 3X3

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O.OEO
21:00' 22:00 ' Time
File:S975815 tl-848 Acq:ll-SEP-1997 03:08:30 EH- Voltage SIR 70S Noise: 811
331.9368 T:2 BSOB(256, 30, -3 .0) PKD( 7,5, 3, 0. 05\, 3244. 0,1 . 00\,F, T) Exp:EPCUS
TRIANGLE LABS Text:TLI M23 BLANK TLI#4308S
1001
80:
60:
40:
20:
0:













' 20:00 '
INJ. TIME - 03:09
A1.49E7 3.8X6
\A1.18X7
ft


I V; v
.3 . 0X6
.2.3X6
.1 . 5X6
.7.6X5
O.OEO
'21:00 	 22:00' ' ' ' Tiae
rile:S975815 #1-848 Acq:ll-SEP-1997 03:08:30 EI+ Voltage SIR 70S Hoise:39
333.9338 T:2 BSUB(256, 30, -3. 0) PKD(7,
5, J, 0.05%, 15ff.O,1.00%,J', T) Exp:EPCUS
TRIANGLE LABS Text:TLI M23 BLANK TLH43085
1001
80:
60-
40:
20.
0






	 19:00 '






20:00
INJ. TIME - OJ.-09
A1.84E7 4.6X6
f\A1.47E7
1 II
ft


; V; V
.3.7X6
'•.2.7E6
Ll . 8E6
.9.1X5
O.OEO
'21:00 	 22:00' ' ' ' TjUie
rile:S975815 tl-848 Acq:ll-SEP-1997 03:08:30 Eli- Voltage SIR 70S Noise: J 8
327.8847 T:2 BSUB( 256,30, -3 . 0) PKD(7,
5,3,0.05\,152.0,1.00%,T,T) Exp:EPCUS
TRIANGLE LABS Text : IX J M23 BLANK TLI#43085
1001
80.
60.
40.
20.
0.






19:00'






'20:00
INJ. TIME - OJ.-09
A2.11E7 5.5X6
I



1 \
.4.4X6
.3.3E6
.2.2X6
.1.1X6
'• O.OEO
21:00 22:00 Time
rile. -S9 75 815 #1-848 .Acsr:ll-Si:j>-1997 03:08:JO EI+ Voltage SIR 70S
330.9792 T:2 ElpiEPCUS

TRIANGLE LABS Text. -HI M23 BLANK TLI#43085
100
80

60
40
20
0
i
m ^_JLAJ^WW*^*'*V^'





' 19',00
20:10
^y-^VWV^V^VVA
\




' 20\00'

UKT. TIMX - 03:09
21^22^0023,20 22OS
j' ^-^"^^A ft f
°130 21:10 -^ III I
yW^'>^'^. *~**^/*~ *v~*r~ ** *»t~j~*>



^.9.4X6
-.7.5X6

.5.7X6
.3.8X6
.1.9X6
• o.oxo
21 : 00 22: 00 Time
49

-------
 HetS975815 11-848 Acq:ll-SXP-1997 03i08i30 SI+ Voltage  SIX  70S Hairnet33
 39.8597 r-.2 BSUB(256,30, -3.0)  PKD(7, 5,3,0.05\,132.0,1.00\,F,T)  KxptXTCUS
TXIAHGLS LABS  TaxtiTLI H23  BLANK  TLI#43085                IKJ. TIMS "   03t09
 OOi,
                                            A5.08X4
 so:
                                                                               26s 00
              23i00                 24,00                25:00
 •ile:S975815 #1-848 Acqill-SEP-1997 03t08s30 XI+  Voltage SIS 70S Noiae:409
 41.8567 T:2 BSO3(256, 30, -3. 0) PKD( 7,5, 3, 0 .OS\,1636.0,1.00\,T, T) XxpiEPCUS
TRIANGLE LABS   Text:TLI H23 SLANT  TLH4308S                 IJKT. TIKE -   03:09
                                      A2.40E4
                                                                               26:00
              23i00                 24:00                25:00
rile:S975815 #1-848 Acq:ll-SEP-1997 03:08:30 EH- Voltage  SIR 70S Noise-.44
351.9000 T:2 BSUB(256,30,-3.0) PKD(7,5,3,0.OS\,176.0,1.00\,T,T)  Exp:EPCUS
TRIANGLE LABS  Text:TLI M23 BLANK  TLIt43085                 IIKT.  TIKE -   03:09
100*                                              A2.24E7         A2.09E7
 sod
 sol
 40:
 20.
  0:
                                                                                                      .7.3X6
                                                                                                      \.5.8X6
                                                                                                      .4.4X6
                                                                                                      .2.9X6
                                                                                                      .1.5X6
                                                                               26:00
               23:00                 24:00                25:00
 rile:S975815 #1-848 Acqsll-SEP-1997 03:08:30 EH- Voltage SIR 70S Noiae:46
 353.8970 F:2 BSUB(256,30,-3.0)  PKD(7,5,3,0.05\,184.0,1.00\,r,T) ExpsEPCUS
 TRIANGLE LABS  Text:TLI M23  BLANK  TLI#43085                INJ. TIMS -   03:09
                                                  A1.32E7        A1.39E7
  ao:
  60:
  40:
  20:
   o.
                                                                                                       .0.0X0
                                                                                                          Tim,
                                                                                                      .4.6X6
                                                                                                      .3. 7X6
                                                                                                      .2.8X6
                                                                                                      .1. 8X6
                                                                                                      .9.2X5
               23:00                 24:00                25:00
 rile:S975815 #1-848 Acq:ll-SEP-1997 03:08:30 EI+ Voltage  SIR  70S
 330.9792 T:2 Exp:EPCUS
 TRIANGLE LABS  Text:TLI M23 BLANK  TLI#43085                INJ. TIMS -
                                             24:23
                                                                               26:00
                                                                                                       0.0X0
                                                                                                          Tia
               23:00                 24:00                25:00
 rile:S975815 #1-848 Acq:ll-SEP-1997 03:08:30 EI+ Voltage SIS 70S
 409.7974 f:2 Exp:XPCUS
 TRIANGLE LABS  Text:TLI H23 BLANK  TLI#43085                INJ. TIMX
 1001
  SO:
                                                                                26:00
                                                                             03:09
               231 00
                                     24:00
                                                           25iOO
                                                                                26 i 00

-------
 'Ue,3975B15  #1-848 Acqtll-sXf-1997  03:08:30 EI+ Volt*ye SXt  70S Ooifm:44S	
 55.8546 r:2  BSUB(256,30,-3.0) PKD(7t5r3,0.05\,17»4.0tL.OO\rr,T) ExptXPCUS
TRIAHGLX LABS  TextiXLJ M23 BLANK  TLIt43085                I JUT. TIME •   03:09
 00\
         24100                         25100                          26'tOO
 ile:S975815 #1-848 Acq:ll-SEP-1997 03,08,30 EI+ Volt* ye  SIS 70S Ho±me,36
 57.8516 Ts2 BSOB(256,30,-3.0)  PKD(7,5,3, 0. 05%, 144.0,1. 00\,r,T) Xxp:XPCOS
TRIANGLE LABS  Text:ITT M23 BLANK  TLI#43085                 IJKT. TIME -   03:09
 OOi                               A1.31X4
                                                            Al. 61E4
                                                                'A2.15E4
                                                                      A7.32E3
         24:00                          25:00                          26:00
r±le:S975815 #1-848 Acq:ll-SEP-1997 03:08:30 EI+  Voltage SIR 70S Wbiae.OP
  67.8949 F:2 BSUB(256, 30,-3 . 0)  PKD( 7, 5, 3, 0. 05\, 156. 0, 1. 00\,T, T) Exp:EPCOS
TRIANGLE LABS  Text-.TLI M23  BLANK  TLI#43085                 JJCJ. TIME  •   03>09
100*                                                           A1.26E7
  80.
  60.
  40:
  20:
                                                                       1.19E6
         24:00                          25:00                          26:00
 rilesS975815 #1-848 Acqsll-SEP-1997 03:08:30  EI+ Voltage SIR  70S Noiae:11
 369.8919 T:2 BSUB(256,30,-3.0) PKD(7,5,3,0.05\, 164.0,1.00\,T,T) Exp:EPCVS
 TRIANGLE LABS   Text:Til H23 BLANK  TLI#43085                 INJ. TIME -   03:09
 1001                                                            A8 $9E6
so:

60:

40.

20:

 0.
                                                                       7.83E5
         24:00                         25:00                          26:00
 F±le,3975815  #1-848 Acqsll-SEP-1997 03:08:30 EH- Voltage  SIR 70S
 330.9792 r:2  XxptXPCUS
 TRIANGLE LABS  Text:TLJ M23 BLANK  TLH43085                 IKT. TIME -   03:09
                                        25:00  25:12 25:25  25:38  ^i*3    26:08
            * wO      j->--i^r**j~\. ' f* 'i-^" *~ jAvy-r^rLfV^'^
  aoJ

  60.

  40.

  20.

    0.
4.1E6

3.3E6

2.5E6

1. 6E6

8.2E5

.O.OEO
    Tim



.2.9E6

.2.3X6

.1. 7E6

.1.2X6

.5.8X5
          24:00
                                         25100
                                                                        26100
 0.0X0
    T±a
.1.2X7

.1. 0X7

.7.5X6

.5.0X6

.2.5X6
.0.0X0
    Tim

-------
rlle,S975815  #1-405 JUaj:ll-srj>-1997 03:08:30 EI+  Voltage SIX 70S Half0:1048
373.8208 r:3  tSUB(256,30, -3. 0) PXD(7,5,3, 0. OS\,4192.0,1.00\,T,T) XxpiXPCUS
TRIANGLE LABS  TexttTLI M23 BLANK  TLIt4308S                 1X7. TIMX "   03:09
10 OS,                               A3.31X4
  27:12  27:24 27^35 27:48  2sl- 00 28:12 28:24  28:36 28148 ' 29: 00' 29:12' 29:24' 29:36'29«48'Joi00' 30*1.2    Timi
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file:S975815  #1-405 Acqtll-SEP-1997 03:08:30 XI+ Voltage SIR 70S Noiae:899
383.8639 F:3  BSUB(256,30,-3.0) PKD(7,5,3,0.05\,3596.0,1.00\,F,T)  Ezp-.XPCUS
TRIANGLE LABS  Tezt:TLI M23  BLANK  TLJ#43085                 INJ.  TIKE -   03:09
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File:S97S815  #1-405 Acq:ll-SEP-1997 03:08:30  EI+  Voltage SIR 70S Noise:985
385.8610 F:3  BSUB( 256, 30,-3 . 0 ) PKD( 7, 5,3, 0 . 05*, 3940 . 0,1. 00%,r, T) Ezp:EPCUS
TRIANGLE LABS  Text.-ZXX M23 BLANK  TLH43085                 INJ. TIME -   03:09
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File:S975815  #1-405 Acq:ll-SEP-1997 03:08:30  EH- Voltage SIR 70S
392.9760 T:3  Xxp:XPCUS
TRIANGLE LABS  Text:TLI M23 BLANK  TLI#43085                 IWJ. TIME -   03:09

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 Tile:S975815 #1-405 Ac^:ll-srP-1997 03:08:30 EI+ Voltage SIX  70S
 445.7555 F:3 Exp:EPCUS
 TRIANGLE LABS  Text:TLI M23 BLANK  TLH43085                JWJ.  TIME -   03:09
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                                                                                                              52

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 91.8127  f:3  BSOB(256,30,-3.0) PKD(7,5,3,0.05\,2424.0,1.00\,r,T) ExptEPCOS
TRIANGLE  LABS  Telt-.TLI H23 BLANK  TLH43085                 INJ. TIME -   03109
  00*                                                      A3.61E4
     27:48   20:00    28:12   28:24    28:36   28:48   29:00    29:12   29:24    29:36
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File:S97S815  #1-430 Acqsll-SEP-1997 03,08,30 EI+ Voltage SIS 70S Noise,230
 09.7789 T:4  BSOB(256,30, -3.0) PKD(7,5,3, 0.05\,920.0,1.00\,r,T) Xxp:SPCOS
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File:S97S815  #1-430 Acqsll-SEP-1997 03,08,30 EH- Voltage SIS  70S  Jfc.iae.-548
417.8253  T:4  BSUB(256, 30, -3. 0) PKD(7,5,3,0 .OS\,2192.0,1.00\,r,T)  Exp-.EPCUS
TRIANGLE  LABS  Tert:TLI M23 BLANK  TLI#43085                INJ.  TIME -   03:09
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 419.8220 T:4 BSOB(256, 30,-3.0 ) PKD( 7, 5, 3, 0. 05\, 1648. 0,1. 00%, T, T) Exp:EPCUS
 TRIANGLE LABS  TextsTLI M23 BLANK  TLI#43085                INJ. TIME -   03:09
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File:S975815 #1-430 Acqsll-SEP-1997 03:08:30 EI+ Voltage SIS 70S
430.9729 F,4 ExpsEPCUS
TRIANGLE LABS  Text-.TLI M23 BLANK  TLI#43085                INJ. TIME -   03:09
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 file:S975815 #1-430 Acq:ll-SEP-1997 03:08,30 EH- Voltage SIS 70S
 479.7165 F,4 Exp:EPCUS
 TRIANGLE LABS  TextsTLI M23  BLANK  TLH43085                1KT. TIKE
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TRIANGLE LABS  Text:TLI M23 BLANK  TLH43085                 JK7.  TIME -   03:09
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TRIANGLE LABS  Text:TLI M23  BLANK  TLIt4308S                INJ. TIME -   03:09
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 Tile:S975815  tl-430 Acq:ll-SEP-1997 03:08:30 Eli- Voltage SIS  70S  Noiaei896
 437.8140 T:4  BSUB(256,30,-3.0) PKD(7,5,3,0.05\,3584.0,1.00\,F,T)  Exp:EPCUS
 TRIANGLE LABS  Text.-IXJ  M23 BLANK  TLI#430S5                INJ.  TIME -   03:09
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 File:S975815 tl-430 Acqtll-SEP-1997 03:08:30 £1* Voltage SIR 70S
 430.9729 F:4 ExptEPCUS
 TRIANGLE LABS  Text:TLI M23  BLANK  TLIt43085                X1KT.  TIME -   03:09
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         31:00             32:00            33:00             34:00             35:00
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 TRIANGLE LABS  Text:TCI M23  BLANK  TLIf43085                INJ. TIME -   03«OS
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 TRIANGLE LABS  Teit:TLI M23 BLANK  TLI#4308S                INT.  TIME -   03:09
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-------
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123.7766 F:4 Exp:EPCUS
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125.7737 F:4 Exp:EPCUS
Sample Text:TLI M23 BLANK  TLI#43085     ,  ,         INJ.  TIME =   03
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-------
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43.7399 F:4 Exp:EPCUS
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-------
TLI Project:      43085                 Method 23 TCDD/TCDF Analysis (DB-225)
Client Sample:   TLI M23 Blank                          Analysis File:   P973852
Client Project:
Sample Matrix:
TLI ID:

Sample Size:
Dry Weight:
GC Column:
S413-004
XAD
TLI Blank

1.000
n/a
DB-225

Date Received:
Date Extracted:
Date Analyzed:
Dilution Factor:
Blank File:
Analyst:

/ /
09/04/97
09/12/97
n/a
P973852
ML

Spike File:
ICal:
ConCal:
% Moisture:
% Lipid:
% Solids:

SPC2NF04
PF22206
P973843
n/a
n/a
n/a
Analytes
Amt. (ng)
Bt
EMPC
Ralfo *
(T Flags
2,3,7,8-TCDF
   ND
0.03
 Internal Standard
Amt.; '(ng>'. ';'-;:;:'vJ4^:;:%:RecoVery';" QC Limits ;; .. • :Ratfo::;'-!f f :h
l3Ci:-2,3,7,8-TCDF
   2.7
   67.4
40%-130%
0.78
                                                                             20:39
 Recovery Standard
                                        Ratio
                                          Slags
 13Cirl,2,3,4-TCDD
                                         0.79
                                                                             19:41
                       Data Reviewer
            Of    I
            VK.L; - L^ i .
                                           Page 1 of 1
                     09/18/97
                                                                               CWF_PSR viOO. LARS 6.10.M
 Triangle Laboratories, Inc.®
 801 Capitola Drive • Durham, North Carolina 27713
 Phone: (919) 544-5729 • Fax: (919) 544-5491
                                               Printed: 15:52

-------
Data Review By:
       Initial   	Date...

         J *"       ( / Kill  Calculated Noise Area:
                                                                       1.53
The Total Area for each peak with an ion abundance ratio outside
ratio limits has been recalculated according to method requirements.
Page No.
09/12/97
         Listing of P973852B.db£
         Hatched GC Peaks / Ratio / Ret. Time
Compound/
M_Z	QC.Log Omit Why ..RT.  OK Ratio Total.Area... Area.Peak.1.. Area.Peak.2..  Rel.RT Confound.Name..  ID..  Flags.
TCDF
304-306
 304-306
               0.65-0.89
DC  NL   0:00     0.87
DC  SN  22:12 RO  1.00
DC  SN  22:16     0.65
      0 Peaks
1.96
0.58
0.91
0.00
0.786-1.096
    0.000
    1.075
    1.078
 13C12-TCDF
 316-318
 316-318
 13C12-TCDD
 332-334
0.65-0.89
DC
DC
DC
DC
DC

DC
DC


DC
DC
NL
WL
WL
WL
WL

SN
WH
1

NL
SN
0:00
19:12
19:21
19:31
19:36
20:39
21:31
22:30
Peak

0:00
18:23
RO
RO
RO
RO


RO
RO

0.
RO
RO
0.
3.
0.
4.
0.
0.
4.
0.

94
77
34
38
86
78
45
93

65-0. 8S
1
1
.39
.33
                                2.25
                                0.23
                                0.92
                                0.42
                                6.26
                              516.62        225.80
                                0.19
                                4.96
                              516.62

                       Above: TCDF  / TCDD Follows -
 332-334
                                                2.11
                                                1.49
                         19:27     0.79         431.45        191.02
                         19:41     0.79         552.23        242.97
                         20:21 RO  0.91          5.26          2.71
                       3 Peaks                 988.94
                              0.952-1.048
                                  0.000
                                  0.930
                                  0.937
                                  0.945
                                  0.949
                          290.82  1.000  13C12-2378-TCDF ISO
                                  1.042
                                  1.090
                                                              0.897-1.103
                                                                  0.000
                                                                  0.945
                                                          240.43  1.000  13C12-2378-TCDD IS1
                                                          309.26  1.012  13C12-1234-TCDD RSI
                                                            2.97  1.046
 Column Description	  "Why" Code Description	   QC  Log Desc.
  M_Z    -Nominal Ion Mass (88)
  ..RT.  -Retention Time  (mm:ss)
  Rat.l  -Ratio  of M/M+2  Ions
  OK    -RO=Ratio Outside Limits
                 WL-Bclow Retention Time Window
                 WH-Above Retention Time Window
                 SN-Below Signal to Noise Level
                  A-Peak Added
                  K-Peak Kept
                  D-Peak Deleted
                                 
-------
     !  K B B 8 8  fi
00

-------
            17tOO         18,00        191 00         20100         21,00
 ±le,P973852 tl-755 Acq,12-SXP-1997 18:30:31  11+ Voltagm SIS 70P No±a»,524
 05.8987 BSUB(256,30,-3.0) PKD(5,3,1,0.10\r 2096.0,0.00\,r,F) Exp,DB225
TXIANGLX LABS  TexttTLI H23  BLANK TLH430B5
                                                     A2.99X3
 il»:P97385J tl-755 Acqtll-SfP-iSS/ 18:20,31  Sir  VOlt*y9 SIS 7OP NOiff,4S7
 03.9016 BSUB(256,30,-3.0) PKD(3,3,1,0.10\,1828.0,0.00\,T,T) XzptDB225
  IANGLX LABS  tuxtiTLI M23 BLANK TLIt43085
 001
221 00
            17,00         18:00         19': 00         30', 00         21:00
r±lesP973852  tl-755 Acq>12-SEP-1997 18:20:31 CI+ Voltage SIS 70P Noise,593
 15.9419 BSUB(256,30,-3.0)  PKD(5,3,1, 0.10\,2372.0,0.00\,T,T) ExpsDB225
TRIANGLE LABS  TeJCttTLI M23 BLANK TLI#43085
 00\                                                          A2.36E6
  so:

  50:

  40:

  20:
221 00
             17,00         18,00         19,00         30,00         21,00
 riletP9738S2 tl-755 Ac
-------
 1J.*:P973852 tl-755 Acqi 12-3KP-1997 18:20:31 XI + Voltage SIX 7OP Boii*l575
 19.8965 BSUB(256,30,-3.0) PXD(5,3,1,0.10\,2300.0,0.00\,T,f) Ixp:DB225
TXIANGLX LABS  TextiXCX M23 BLANK TLH43085
 004                                    A5.63E3
                   18.00              19:00             20.00             21:00
 •ile:P973852 #1-755 Acq:12-SXP-1997 18:20:31 XI* Voltage SIX  70P Nolle:465
 21.8936 BSOB(256,30,-3.0)  PKD(5,3,1,0.10\,1860.0,0.00\,T,T)  Exp:DB225
TXIANGLX LABS  TeitsTLI M23 BLANK TLH43085
 80.
 60.
 40.
     A5.29K
                                                                                             22100
                   18:00              19:00             20:00             21:00
rile:P9738S2 #1-755  Acqtl2-SEP-1997 18:20:31  EI+  Voltage SIX 70P Noiee:443
 '27.8847 BSOB(256,30,-3.0) PKD(5,3,1,0.10\,1772.0,0.00\,T,T) Exp:DB225
TRIANGLE LABS  TeltiTLI H23 BLANK TLH43085
 1001                                        A3.51E6
  80.

  so:

  40:

  20.
                    18:00             19:00             20:00              21:00
 F±le:P973852 #1-755 Aoj:12-SEP-1997 18:20:31 EH- Voltage SIX 70P Noiee:826
 331.9368 BSDB(256,30,-3.0) PKD(S,3,1, 0.10\,3304. 0, 0.00\rT,T) Exp:DB225
 TRIANGLE LABS  TextlTLI M23 BLANK TLH43085
 100*                                             A2.43E6
  80.


  60.

  40.


  20.
   OJ
A1.91E6
                     T
                                                          T
                                                                            T
                    18:00              19:00              20:00             21:00
 Tile:P9738S2 #1-755 Acq:12-SEP-1997 18:20:31 EI+ Voltage SIX 70P Soi»e:594
 333.9338 BSUB(2S6,30,-3.0)  PKD(S, 3,1, 0.101,2376. 0, 0.00\,T,f) Eip:DB225
 TRIANGLE LABS  TextsTLX H23 BLANK TLIt430S5
 1003,                                             A3. OSES
  80.

  60.

  40.

  20.

    0.
                                       19:00
           20':00'
31(00'
                                                .2.2; 00
                                                22s 00
                                                22': oo'
                                                                                              22:00
                                                        '.4.1X3

                                                        .3.1X3

                                                        .2.0X3

                                                        .1.0X3

                                                         O.Ott
                                                        .9.5X5

                                                        -7.6E5

                                                         .5.7E5

                                                         .3. BES

                                                         '.1.9X5
                           O.OEO
                               Tim.
                           .6.8X5

                           .5.4X5

                           ".4.1X5

                           '.2.7X5

                           11.4X5

                           .0.0X0
                                                         .8.4X5

                                                         .6.7X5

                                                         '.5.0X5

                                                         '.3.3X5

                                                         .1. 7X5
O.OEO
   Time
                                                                                                             70

-------
rilezf973852 #1-755 Ao»»12-S*P-1997 lfl.20.Jl 11+ Voltage SIM 70P
303.9016 XxpiDB235
TRIANGLE LABS  TexttTLI M23 BLANK TLH43085
100J
 80:
 60:
 40:
 201
       16 40                                                       31l0ai'3a                   I1'0*'
    *w¥vt^
             T
                           T
                                        -r
                                                      -r
                                                                   T
            i?', oo        le'too         191 oo        ao'too         aitoo
FiletP973853 11-755 Acqil3-SEP-1997 18:20:31 EH- Voltage SIX 70P
315.9419 Exp:DB225
TRIANGLE LABS  TexttTLI M23 BLANK TLI*43085
1004
 aol
 60l
 40:
 ao:
                                                                               'aa'too
            17:00         18:00        19:00         20:00         21:00         22:00
rile>P973853 #1-755 Acqtl3-SEP-1997  18>30>31 EI+ Voltage SIR  70P
319.8965 Exp:DB325
TRIANGLE LABS  TeitiTLI M33 BLANK TLH4308S
             17:00         ISl-OO         1S:00         20l-00         21:00
 r±leiP973852 #1-755 Acqil3-SEP-1997 18t20i31 EI+ Voltage SIR 70P
 331.9368 Exp:DB235
 TRIANGLE LABS  TextiTLI M23 BLANK TLH43085
 1001                                            19141
                                                                               22:00
  80:
  60.
  40:
  20:
                                              19,27
            17:00        18:00         19:00        20.-00         21:00        22:00
J-ile:P973852 #1-755 Acqtl2-SEP-1997 18:20:31 EI+ Voltage SIR TOP
292.9825 Eip:DB225
TRIANGLE LABS  Text-.TLI M23 BLANK TLIt43085
                               18:26
    -~~****r~*~~~^jf^--^tt-^*~rv
  80:
  60:
  40:
  20:
                                                                                                 1X3
                                                                                              -.4.1X3
                                                                                              .2.0X3
                                                                                               0.0X0
                                                                                               6.4X5
                                                                                               5.1X5
                                                                                               3. 8X5
                                                                                              .2.6X5
                                                                                              .1.3X5
                                                                                                .0.0X0
                                                                                                    Time
                                                                                               .0.0X0
                                                                                                   Time
                                                                                                6.8X5
                                                                                                5.5E5
                                                                                                4.1X5
                                                                                                2.7X5
                                                                                                1.4X5
                                                                                                 O.OEO
                                                                                                    T±me
                                                                                                 6.2X6
                                                                                                 5.0X6
                                                                                                 3.7E6
                                                                                                 .3.5X6
                                                                                                 -.1.2X6


17:00
F±le:P973852 #1-755
33 0.9 792 Exp:DB225

18:00
AC9.-12-SEP-1997


19:00

20:00 21:00 22

0.0£0
1 00 Time
18: 20! 31 EH- Voltage SIR TOP



TRIANGLE LABS TexttTLI M23 BLANK TLH43085
1001
so:
60:
40:
20.
0.
^~**iii£L17'10
L*J 1 I'^IMA^^




17:00
18:24
\*+^*m~*\**r~ ' "*-> '•




18:00
19,13
\f~A****f*'Mfw**




19:00
19:38 20:09 21:15
•~~w>«/*v
-------
Ref, uss   232,9825     Peak top
Helpjt  1,86 volts  Spai   286 ppi
       file naie
Data   fllenaie
Resolution
Group nuiber
lonlzatlon wde
Sultchlng
Ref, lasses   292,9825,
 fl  292,9825
 6  383,9816
    C4AC 0001
    OW.WO/
 D  315.9419
 E  317,9389
 F  319,8965
 G  321,8936
 H  327,8847
 I  338,9792
J
K
L
H
       1
     El*
 VIM
388.9761
336,9792
331,9368
333,9338
375,8364
 Chamd.   I  338,9792     Peak top
 Hel^t  1,85 volts  Span   208 ppi
                                                                                72

-------
TLI Project:      43085
Client Sample:   O-M23-1
Method 23 PCDD/PCDF Analysis (a)
             Analysis File:  S975866
Client Project:
Sample Matrix:
TLI ID:

Sample Size:
Dry Weight:
GC Column:
S413-004
M23Train
181-55-1ABE

1.000
n/a
DB-5

Date Received:
Date Extracted:
Date Analyzed:
Dilution Factor:
Blank File:
Analyst:

09/03/97
09/04/97
09/13/97
n/a
S975815
ML

Spike File:
ICal:
ConCal:
% Moisture:
% Lipid:
% Solids:

SPX23704
SF56117
S975861
n/a
n/a
n/a
Artalytes
2,3,7,8-TCDD
1,2,3,7,8-PeCDD
1,2,3,4,7,8-HxCDD
1,2,3,6,7,8-HxCDD
1,2,3,7,8,9-HxCDD
1,2,3,4,6,7,8-HpCDD
1,2,3,4,6,7,8,9-OCDD
2,3,7,8-TCDF
1,2,3,7,8-PeCDF
2,3,4,7,8-PeCDF
1,2,3,4,7,8-HxCDF
1,2,3,6,7,8-HxCDF
2,3,4,6,7,8-HxCDF
1,2,3,7,8,9-HxCDF
1,2,3,4,6,7,8-HpCDF
1,2,3,4,7,8,9-HpCDF
1,2,3,4,6,7,8,9-OCDF
;^otatev..kv.,.^^|'^-:
Total TCDD
Total PeCDD
Total HxCDD
Total HpCDD
Total TCDF
Total PeCDF
Total HxCDF
Total HpCDF
Amt* (ng)
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
^•^.Arot-.CngT
ND
EMPC
ND
ND
0.15
ND
ND
ND
DL EMPC
0.09
0.1
0.1
0.1
0.1
0.2
0.5
0.08
0.09
0.09
0.09
0.07
0.09
0.1
0.1
0.2
0.4
^.;»«infa«fc;;l»,^:iMPC
0.09
0.53
0.1
0.2
1
0.09
0.09
0.2
Raffo HT Ffegs






—



	





—
Flags



—



. 	
                                        Page 1 of 2
                           X237.PSR vlOO. LARS 6.10.C
 Triangle Laboratories, Inc.®
 801 Caprtola Drive • Durham, North Carolina 27713
 Phone: (919) 544-5729 • Fax: (919) 544-5491
                        Printed: 15:16 09/17/9

-------
                                            lental Services
TLI Project:     43085
Client Sample:   O-M23-1
Method 23 PCDD/PCDF Analysis (a)
             Analysis File:  S975866
internal Standards
13C12-2,3,7,8-TCDF
13C12-2,3,7,8-TCDD
13C12-l,2,3,7,8-PeCDF
13C12-l,2,3,7,8-PeCDD
13C12-l,2,3,6,7,8-HxCDF
13C12-l,2,3,6,7,8-HxCDD
13C12-l,2,3,4,6,7,8-HpCDF
I3C12-1,2,3,4,6,7,8-HPCDD
13C,2-U,3,4,6,7,8,9-OCDD
Surrogate Standards (Type A)
37CL,-2,3,7,8-TCDD
'3C,2-2,3,4,7,8-PeCDF
13Ci2-l,2,3,4,7,8-HxCDF
l3Ci2-l,2.3,4,7,8-HxCDD
l3C,2-l,2,3,4,7,8,9-HpCDF
Alternate Standards (Type A)
l3Cu-l,2,3,7,8,9-HxCDF
l3C,2-2,3A6,7,8-HxCDF
Recovery Standards; ..:
13C,2-1(2,3,4-TCDD
13Ci2-l,2,3,7,8,9-HxCDD
Ami (ng)
5.5
5.8
6.4
7.1
4.9
4.9
3.6
3.5
4.8
Anrrt. (ng)
3.2
2.9
3.0
2.6
3.1
Amt (ng) ;?
3.0
3.7



% Recovery "
137
145
160
111
124
122
91.2
88.5
60.5
-:'!' ^Recovery
79.3
71.8
73.8
64.4
78.7
&$$***&£:.
74.3
92.3



QC Limits
40%-130%
40%-130%
40%-130%
40%- 130%
40%- 130%
40%- 130%
25%-130%
25%-130%
25%-130%
QC Limits
70%- 140%
70%- 140%
70%- 140%
70%- 140%
70%- 140%
QC Limits
40%- 130%
40%-130%



Ratio
0.80
0.78
1.23
1.46
0.51
1.19
0.43
1.02
1.00
Ratio ?;.P

1.41
0.52
1.21
0.44
; Ratfo %
0.52
0.50
. Ratio
0 84
1.23
RT
23:17
23:47
26:29
27-24
29:38
30-16
32-06

35:22
;?*rr,fj!
23-48
27-06
29:33
30-12
33:14
:,m • ,-.
30:45
30:05
RT

30:32
Flags

—
RO

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v

Ffegs
Q 	
Flags

"-
                     Data Reviewer

                                       Page 2 of2
Triangle Laboratories, Inc.®
801 Capitola Drive • Durham, North Carolina 27713
Phone: (919) 544-5729 • Fax: (919) 544-5491
                                                           09/17/97
                                                                         X237_PSRY2.00,U«S 6.10.04
                      Printed: 15:1609/1*

-------
Daca Review By:
       Initial    ....Date...

         y._       I /  I-**/ / T" calculated Noise Area:
                                                                       1.69
The Total Area for  each peak with an ion abundance ratio outside
ratio limits has  been  recalculated according to method requirements.
Page No.
09/17/97
        Listing of S975866B.dbf
        Matched GC Peaks / Ratio /  Ret. Time
Compound/
M_Z.... QC.Log Omit Why ..RT.  OK Ratio Total.Area... Area.Peak.1.,
TCDP
304-306
        D

        D

        D
 304-306
0.65-0.89
DC
DC
DC
DC
DC
DC
DC
DC
DC

DC

NL
WL
WL
WL
SK
SN
SN
SN
SN

SN
1
0:
18:
19:
19:
19:
19:
20;
21
21
22
22
00
34
02
19
:33
49
:02
:24
:52
:05
:26
RO
RO
RO
RO
RO
RO
RO
RO
RO

RO
0.
1.
0.
3.
4.
a.
2.
1.
0.
0.
0,
94
47
51
29
89
59
73
11
92
,78
.94
Peak
0.
1.
1.
0.
3.
1.
4.
3.
5,
8
5
8
28
66
36
60
17
95
.94
,72
.15
.27
.06
.27
                                             3.62
Area.Peak.2..  Rel.RT Compound.Name..  ID..  Flags.

           0.838-1.092
               0.000
               0.805
               0.826
               0.838
               0.848
               0.860
               0.869
               0.928
               0.949
          4.65  0.958
               0.973
 13C12-TCDF
 316-318
         MKT
 316-318
               0.65-0.89
DC  NL   0:00 RO  1.86          0.39
DC  WL  18:57 RO  0. 50          1.56
DC  SN  22:25 RO  1.91          2.67
DC  SN  22:46 RO 10.08          0.71
        23:17     0.80        176.80
      1 Peak                  176.80
                                                             78.80
            0.954-1.046
                0.000
                0.822
                0.973
                0.988
         98.00  1.000  13C12-2378-TCDF  ISO
                                       Above: TCDF / TCDD Follows
 TCDD
 320-322
  320-322
0.65-0.89
DC
DC
DC
DC
DC
DC
DC
DC
DC
DC
DC
DC
DC
DC
DC
DC

NL
WL
WL
WL
WL
WL
WL
SN
SN
SN
SN
SN
SN
SN
SN
SN
0
0:
19:
20:
20:
20:
20:
20
21
21
21
21
22
22
22
22
23
00
54
01
17
: 30
:33
:47
:07
:20
:26
:46
:23
:47
-.54
:59
:39
RO
RO
RO
RO
RO
RO
RO
RO
RO
RO
RO
RO
RO
RO
RO
RO
1.
1.
0.
4.
3
1
0
0
0
0
1
1
0
2
2
3
09
43
97
.88
.70
.27
.45
.58
.52
.92
.60
.57
.44
.65
.88
.30
Peaks
                                0.62
                                0.90
                                1.89
                                0.42
                                0.35
                                0.46
                                0.83
                                2.00
                                0.80
                                                   85
                                                   66
                                                 0.50
                                                 1.01
                                                 0.55
                                                 0.92
                                                 0.65
                                                 0.00
            0.875-1.055
                0.000
                0.837
                0.842
                0.853
                0.862
                0.864
                0.874
                0.888
                0.897
                0.901
                0.915
                0.
                0.
                0.
                0.
                                                                   .941
                                                                   .958
                                                                   .963
                                                                   .966
                                                                  0.994
 Triangle Laboratories, Inc.®  Analytical Services Division
 801  Capftola Drive • Durham, North Carolina 27713
 Phone: (919) 544-5729 • Fax: (919) 544-5491
                                                                                        15:16

-------
Page No.
09/17/97
Listing  of  S975866B.dbf
Matched  GC  Peaks / Ratio
/ Rat. Tina
Compound/
M_2.... QC.Log omit Why  ..RT. OK Ratio Total.Area,..  Area.Peak.1..  Area.Peak.2. .  Ral.RT Compound.Name..  ID.. Flags.
37C1-TCDD
328
























0.910-1.090
DC
DC
DC
DC
DC
DC
DC
DC
DC
DC
DC
DC
DC
DC
DC
DC
DC
DC
DC
DC
DC
DC
DC
DC

NL
WL
ML
WL
WL
WL
WL
WL
WL
WL
WL
WL
WL
SN
SN
SN
SN
SN
SN
SN
SN
SN
SN
SN

0:
19:
19:
19:
20:
20:
20:
20:
20:
20:
20:
21:
21:
21:
21:
21:
21:
22:
22:
22:
00
30
45
57
10
10
25
30
41
53
55
15
29
40
43
43
59
19
28
37


0.
11
0.43
6.06


































22:47
22:53
23:07
23;
23:
;29
:39
0.
0.
1.
0.
1.
0.
2.
1.
1.
1.
1.
0.
0.
0.
0.
0.
0.
51
35
06
38
04
96
42
16
13
10
01
38
40
41
78
59
72
0.74
0.67
1.03
0.11
7.13 7.13
23:48
328
13C12-TCDD
332-334












332-334
PeCDF
340-342




2
Peaks
101.18 101.18
0.000
0.
0.
0.
0.
0.
0.
0.
0.
0.
0.
0.
0.
0.
0.
0.
0.
0.
0.
0.
0.
0.
820
830
839
848
848
858
862
870
878
879
893
903
911
913
913
924
938
945
951
958
962
0.972
0.987
0.994
1
.001 37C1-TCDD SUR1
108.31
0.65-0.89
DC
DC
DC
DC
DC
DC
DC
DC
DC
DC
DC



NL
WL
WL
WL
WL
WL
WL
SN
SN
SN
SN


2
0
20
20
20
21
21
21
22
22
22
23
23
23
:00
:08
:24
:58
:03
:11
:29
:07
:30
:37
:28
:37
:47
0.
RO 1.
RO 1.
RO 0.
RO 0
RO 1
RO 3
RO 3
0
RO 2
RO 1
0
0
Peaks
82
.98
,45
.28
.12
.48
.37
.95
.88
.22
.21
.84
.78

1.32-1.78
DC
DC
DC
DC
NL
WL
WL
WL
0:00
23
23
:40
:54
24:05
RO 0
RO 0
RO 0
RO 0
.92
.28
.53
.63
0.31
1
1
0
0
0
0
0
1
0
3
98
151
.04
.45
.64
.18
.44
.87
.37
.09
.32
.40
.04 44.64
.41 66.29
0.910-1.090
0.000
0. 347
0
0
0
0
0
0
0
0
0
53.40 0
85.12 1
.858
.882
.385
.391
.903
.930
.946
.951
.987
.993 13C12-1234-TCDD RSI
.000 13C12-2378-TCDD IS1
249.45

0
4
.20
.49
0.53
1
.35
0.915-1.074
0
0
.000
.865
0.873
0.880
Triangle Laboratories, Inc.® Analytical Services Division
801 Capitola Drive • Durham, North Carolina 27713
Phone: (919) 544-5729 • Fax: (919) 544-5491
                                                                    Printed: 15:16 
-------
Page No.
09/17/97
Listing  of  S975866B.dbf
Hatched  GC  Peaks / Ratio / Ret. Time
Compound/
M_Z....  QC.Log Omit Why
.RT.  OK Ratio  Total.Area...  Area.Peak.1.. Area.Peak.2.. Rel.RT Compound.Name..  ID.. Flags.
 340-342
 13C12-P6CDF
 352-354
        NM
        N
        N
 352-354
 PeCDD
 356-358
 356-358
  13C12-PeCDD
  368-370
         N
         N
  368-370
  HxCDF
  374-376
  374-376
DC WL 24:24 RO 0.57
DC WL 24:54 RO 2.04
DC SN 25:22 RO 2.12
DC SN 25:48 RO 7.75
DC SN 26:32 RO 0.24
DC SN 26:47 1.38
DC SN 27:16 RO . 0.59
DC SN 27:27 RO 2.23
0 Peaks
1.32-1.78
DC NL 0:00 RO 1.09
DC SN 23:32 RO 1.29
23:40 RO 0.72
DC SN 24:09 RO 0.77
DC SN 24:33 RO 2.38
DC SN 25:27 RO 0.63
DC SN 25:46 1.68
DC SN 26:01 RO 0.55
26:29 RO 1.23
27:06 1.41
DC SN 27:22 RO 0.79
3 Peaks

1.32-1.78
DC NL 0:00 RO 1.20
DC WL 24:59 RO 0.81
DC SN 25:41 RO 4.11
DC SN 26:21 1.55
26:32 RO 2.90
1 Peak
1.32-1.78
DC NL 0:00 1.56
DC SN 25:53 RO 0.74
26:32 RO 0.70
27:24 1.46
2'V':"30 RO 1.03
3 Peaks

1.05-1.43
DC NL 0:00 RO 0.96
DC WL 28:42 RO 1.57
DC WL 28:49 RO 2.33
DC SN 30:16 RO 1.55
DC SN 30:41 1.17
0 Peaks
0.99
7.75
0.87
0.82
7.55
1.12
0.87
1.22
0.00

0.20
0.72
7.44 4.52
0.66
0.66
0.90
2.98
1.04
177.68 108.00
123.73 72.49
2.65
308.85


0.20
1.30
1.66
2.40
18.28 20.78
18.28

0.23
2.35
12.91 7.85
110.12 65.30
11.68 7.10
134.71


3.96
2.26
5.42
1.93
2.95
0.00
0.892
0.910
0.927
0.943
0.970
0.979
0.996
1.003

0.844-1.156
0.000
0.860
6.26 0.865
0.882
0.897
0.930
0.942
0.951
37.70 0.968 13C12-PeCDF 123 IS2
51.24 0.990 13C12-P6CDF 234 SUR2
1.000


0.926-1.024
0.000
0.908
0.934
0.958
7.17 0.965

0.850-1.150
0.000
0.941
11.26 0.965
44.82 0.996 13C12-PeCDD 123 IS3
6.86 1.000


0.959-1.050
0.000
0.954
0.958
1.006
1.020

 Triangle Laboratories, Inc.®  Analytical Services Division
 801  Capftola Drive • Durham, North Carolina 27713
 Phone: (919) 544-5729 • Fax: (919) 544-5491
                                                                      Flirted: 15:16

-------
 Page No.
 09/17/97
Listing of S975866B.db£
Hatched GC Peaks /  Ratio / Ret. Tina
 Compound/
 M_Z	 QC.Log omit Why ..RT. OK Ratio Total.Area... Area.Peak.1.. Area.Peak.2.. Rel.RT Confound.Name..  ID.
                                                                              Flags.
13C12-HXCDF
384-386



N
N


N
N
N
384-386
HxCDD
390-392




390-392
13C12-HXCDD
402-404








N
N
N

402-404
HpCDF
408-410
408-410
13C12-HpCDF
418-420





DC
DC
DC



DC
DC
DC




DC
DC
DC
DC
DC


DC
DC
DC
DC
DC
DC
DC
DC
DC






DC


DC


DC
DC

NL
SN
SN



SN
SN
SN


5

NL
WL
SN
SN
SN
0

NL
WL
WL
WL
WL
WL
SN
SN
SN




4

NL
0

NL


SN
SN

0:00
28:33
28:40
28:50
29:33
29:38
29:50
29:53
29:58
30:05
30:45
Peaks

0:00
28:48
29:55
30:01
30:44
Peaks

0:00
28:49
29:04
29:16
29:21
29:27
29:41
29:49
29:53
30:12
30:16
30:32
30:45
Peaks

0:00
Peaks

0:00
32:06
32:24
32:50
32:54
0.
RO
RO

RO


RO
RO
RO
43-0.59
0.
2.
0.
0.
0.
0.
0.
3.
1.
89
57
46
69
52
51
77
57
00
0.50


1.
RO

RO
RO
RO

1.

RO
RO
RO

RO
RO
RO
RO





0,


0
RO

RO

RO
0.

52

3.
0.
2.
8.
104.
147.
0.
0.
1.
102.
71.
434.
Uvrr\t
05-1.43
1.
1,
.04
.16
0.46
0.29
1

.02

3.
3.
1.
0.
4
0
88
82
40
02 3.67
54 35.91
69 49.82
59
32
66
23 33.98
53 24.50
01

.63
.88
.97
.94
.10
.00
05-1.43
1
1
2
4
1
0
3
0
1
1
1
1
1

.12
.64
.93
.32
.35
.51
.41
.93
.49
.21
.19
.23
.34

3
13
1
1
2
1
1
1
3
75
120
99
10
306
u+rS*r\
.88-1.20
0

.37
1
0
1
0
0
.99

-0.51
.19
.43
.25
.45
.65
3
0
.39
.66
.93
.12
.77
.93
.81
.37
.02
.64 41.38
.70 65.47
.30 54.81
.71 6.14
.35

.54
.00
0.863-1.137
0.
0.
0.
5.31 0.
68.63 0.
97.87 0.
0.
0.
0.
68.25 1.
47.03 1.

000
949
953
958
982 13C12-HXCDF
985 13C12-HXCDF
992
993
996
000 13C12-HXCDF
022 13C12-HXCDF





478 SUR3
678 IS4



234 ALT2
789 ALT1

0.953-1.014
0.
0.
0.
0.
1.

000
943
980
983
007







0.967-1.033
0.
0.
0.
0.
0.
0.
0.
0.
0
34.26 0.
55.23 0
44.49 1
4 . 57 1

000
.944
.952
.959
.961
.965
.972
.977
.979
.989 13C12-HXCDD
.991 13C12-HXCDD
.000 13C12-HXCDD
.007










478 SUR4
678 IS5
789 RS2


0.995-1.042
0

.000



0.937-1,125
2
80
6
2
2
.39
.36 24.04
.29 5.48
.49
.10
0
56.32 1
4.37 1
1
1
.000
.000 13C12-HpCDF
.009
.023
.025

678 IS6



Triangle Laboratories, Inc.® Analytical Services Division
801 Caprtola Drive • Durham, North Carolina 27713
Phone: (919) 544-5729 • Fax: (919) 544-5491
                                                                   Printed: 15:16
97

-------
Page No.
09/17/97
Listing  of S975866B.dbf
Matched  GC Peaks / Ratio /  Ret. Tim*
Compound/
M_Z....  QC.Log Omit Why ..RT.  OK Ratio Total.Area...  Area.Peak.1.. Area.Peak.2.. Rel.RT Compound.Name..  ID.. Flags.
        N
418-420
HpCDD
424-426
 424-426

 13C12-HpCDD
 436-438
 436-438
 OCDF
 442-444
 442-444
 OCDD
 458-460
  458-460
  13C12-OCDD
  470-472
  470-472
DC
DC
DC
DC
DC
DC
33:14
SN 33:32 RO
3 Peaks
0.44
2.95
kl»A..A .
0.88-1.20
NL 0:00 1.09
SN 32:12 RO 1.47
SN 32:19 RO 0.72
SN 32:24 RO 0.78
WH 33:11 RO 0.51
0 Peaks
48.74 14.81
1.90
135.39
Ur\/"*TM7 / Ut^*^r> l?i-*l 1 /M*fA
2.24
2.41
1.53
5.16
1.71
0.00
0.88-1.20
DC
DC

DC




DC
DC
DC
DC

DC
DC
DC
DC
DC


DC
DC
DC
DC
DC


DC

DC
DC

NL
SN

SN
1



NL
SN
SN
SN

SN
SN
SN
SN
SN
1

NL
SN
SN
SN
SN
0

NL

WH
WH
1
0:
00 RO
32:24 RO
32:
33:
52

05 RO
2.
0.
1.
0.
68
60
02
77
Peak



0:
31:
31:
32:
32:
33:
33:
33:
34:
35:



00
31
43
02
22
19
31
54
26
:26


0.
RO

RO
RO
RO

RO
RO
RO



76-
0.
0.
1.
0.
0.
0.
0.
0.
5,
0
- Above:
1.02
74
93
12
57
48
97
53
,70
.03
.89
Peak

0
35
35
35
35

-.00
:06
:14
:26
:44
0.
RO
RO
RO
RO

.76'
0
0
3
4
0
-1.02
.63
.49
.09
.57
.98
Peaks

0
35
35
35

:00
:22
:36
:47
0
RO

RO
RO
.76
0
1
-1.02
.28
.00
0.24
1
.22
Peak
0.90
4.30
71.64 36.09
0.96
71.
HpCDD

1.
0.
1.
1.
5.
2.
2.
4.
0.
2.
5.
64
/ Octa-CDD and CDF

72
89
38
30
59 2.63
21
70
99
59
80
,59
33.93 1.035 13C12-HpCDF 789 SUR5
1.045
0.977-1.005
0.000
0.980
0.983
0.986
1.010
0.969-1.031
0.
0.
35.55 1.
1.



0.387-
0.
0.
0.
0.
5.49 0.
0.
0.
000
936
000 13C12-HpCDD 678 IS7
007



1.113
000
891
897
906
915
942
948
0.959
0,
1

.974
.002

0.887-1.113
0.96
0
0
1
1
0
.96
.21
.02
.80
.00
0
0
0
1
1

.000
.992
.996
.002 OCDD AN
.010

0.996-1.005
0
62
0
0
62
.23
.34 31.22
.91
.85
.34
0
31.12 1
1
1

.000
.000 13C12-OCDD ISS
.007
.012

 Triangle Laboratories, Inc.®  Analytical Services Division
 801 Caprtola Drive • Durham, North Carolina 27713
 Phone: (919) 544-5729 • Fax: (919) 544-5491
                                                                      Printed 15:16

-------
Page No.      6           Listing of S975866B.dbf
09/17/97                 Hatched OC Peaks /  Ratio  / Ret. Tine

Compound/
M_Z	 QC.Log Omit Why ..RT. OK Ratio Total.Area... Area.Peak.1..  Area.Peak.2..  Rel.RT Compound.Name..  ID..  Flags.
Column Description	  "Why" Code Description	  QC Log Desc.
H_Z   -Nominal  Ion Hass(es)     WL-Below Retention Time Window   A-Peak Added
..RT. -Retention Time  (mn:ss)   WH-Above Retention Time Window   K-Peak Kept
Rat.l -Ratio of M/M+2  Ions      SN-Below Signal to Noise Level   D-Peak, Deleted
OK    -RO=Racio Outside Limits  
-------
rile:S975S66 tl-905 Acq>13-SXP-1997 Oli33i37 EI+ Voltage SIX  703 Boime:75
303.9016 Tt2 BSUB(256,30, -3.0) PXD<9,S,5, 0.05%,300.0,1.00\,T, T)  ExpiEPCDS
TSIANGLX LABS  TexttO-M23-l TLHH30B5                       1X7. TIMS "   01:36
                 19:00            20:00            21:00            22:00
r±le:S975866 tl-905 Aoq:13-SEP-1997 01:33:37 SI+  Voltage SIS  70S Noise:82
305.8987 T:2 BSUB(256,30,-3.0) PKD(9,5t5,0.05%,328.0,1.00\,F,T) fxptSPCOS
TRIANGLE LABS  Tejct:0-M23-l  TLIt43085                       UKT. TIMS -
100J

  80:
                                                                                     231 00
                                                                            Olt36
                  19:00            20:00           21:00            22:00            23:00
 File:S975866 tl-905 Acq:13-SEP-1997 01:33:37 EI+ Voltage SIR 70S Noiae:203
 315.9419 T:2 BSUB(256,30,-3.0)  PKD(9,5,5,0.05\,812.0,1.00\,r,T) Eip:EPCUS
 TRIANGLE LABS  Text:O-M23-l  TLIt43085                       XK7. TIME -   01:36
 1004                                                                                    A7.90E5
  40:

  20:
                 	1	,	r—i	f	1  'i   I   i'  I   i	1	1	1	1—.	r—T	1« -i  • f • i •""< -T- |" i
                 ISiOO           20:00           21:00            22:00            23:00
 File:S975866 tl-905 Acg:13-SEP-1997 01:33:37 EI+ Voltage SIR 70S Noiae:112
 317.9389 F:2 BSUB(256, 30,-3.0 )  PKD(9, 5,5, 0. 05%, 446. 0,1. 00\,r, T) Exp:EPCUS
 TRIANGLE LABS  Text:O-M23-l  TLIt43085                       IK7. TIME  -    01:36
 1001

  80:

  60:

  40:

  20.
                                                                                                       .2.7X5

                                                                                                       .2.2ES

                                                                                                       .1. 6E5

                                                                                                       .1.115

                                                                                                       .5. 4X4
                                     -r
                                                                      rr
                                                                                                       .o.oro
                                                                                                           Time
                                                                                                        3.4E5

                                                                                                        .2.7E5

                                                                                                        .2.0E5

                                                                                                        .1.4E5

                                                                                                        .6.8E4
                  19:00             20:00            21:00            22:00            23:00
  F±le:S975866 tl-905 Acq:13-SEP-1997 01:33:37 Ell- Voltage SIX 70S
  330.9792 T:2 Eip:EPCUS
  TRIANGLE LABS  Text:O-M23-l TLI143085                       ISJ. TIHE  -    01:36
                                                                                                       .o.oro
                                                                                                           Time
                                    20s00            21:00            22:00
  rile:S975866 tl-905 Acq:13-SEP-1997 01:33:37 EI+  Voltage SIR  70S
  375.8364 T:2 Exp:EPCUS
  TRIANGLE LABS  Text:0-M23-l TLIt43085                       IXJ.  TIMS -   01:36
                                                                                      231 00
                                                                                                        .O.OEO
                                                                                                            Time

-------
 ±10,3975866 fl-905 Acqtl3-SXP-1997 01,33,37 XX+ Volt*f» SIX 70S Half*t192
 19.8965 Ti2 BSU*(256,30f-3.0) PKS(7, 5,3, 0.05\,768.0,1.00\,r,T) XxpiMTCUS
TSIANGLX LABS  T«xt»O-K3J-l TUI43085                       OKT. TIM* •   Oil36
 OC
            20tOO                21', 00                22100                23,00
 ile:S97S866 il-905 Acqtl3-SXP-1997 01,33,37 XI*  Volt*?*  SIM 70S Hoi**t175
 21.8936 n2 BSUB(256,30,-3.0) PXD(7,5,3,0.05\,700.0,1.00\,r,T)  XxpiEfCUS
TSIANGLE LABS  TextiO-M23-l TLI»43085                       ISJ. TIME -   Oil36
  003

  sol

  60:

  40.

  20:

   0:
A1.07E4
                                  Al.
                  A9.65X3
                                       1X4
A4.82X3
      IA9.35X3
                                               A9.37E3
                                                           Al. 01X4
                                                                       A1.95X3
                                 51:00                22:00
F±leiS97S866  fl-905 Acqsl3-SEP-1997 Ols33i37 JTJ+ Volttya SIX 70S Koi*«,69
  31.9368 T,2  BSUS(256,30,-3.0)  PKD(7,5,3,0.05\,276.0,1.00\,r,T) XxpsEPCOS
TRIANGLE LABS  Text:O-M23-l TLH43085                       ISJ. TIME »
1001

  80:

  60:

  401

  20:

   0.
                                                                23,00


                                                                01,36
            20,00                21:00                22:00
 File,S975866 tl-905 Acq:13-SEP-1997 01:33:37 EI+ Voltage SIS 70S JK>isei84
 333.9338 T:2 BSUB(256,30,-3.0) PKD(7,5,3,0.051,336.0,1.00\,T,T) Exp:EPCUS
 TKIANSLE LABS  Text:0-M23-l TLH43085                       XWT. TIME -
 1001

  80:

  60:

  40:

  20:

   o:
                                                                23:00


                                                                01:36
             20:00                 21:00                22:00
 rile:S975866 fl-905 Acq:13-SEP-1997  01:33:37 EH- Voltage SIS  70S Noiae:55
 327.8847 F:2 BSUB(256,30,-3.0) PKS(7,5,3,0.05\,220.0,1.00\,T,T) ExpiEPCUS
 TKIAffSLE LABS  T&ft:O-M23-l TLI#4308S                       HKT. TIMS -
 1003

  aol

  60:

  40:

  20:

   o.
                                                                            23:00
                                                                 01,36
             20:00                21:00                22:00
 Tile:S975866 tl-905 Acqsl3-SEP-1997 01:33:37 EH- Voltage SIS 70S
 330.9792 F:2 Exp:EPCUS
 TRIANGLE LABS  Text,O-M23-l  TLH4308S                       XK7. TIME
 100\
   80:

   60:

   40:

   20:

    o:
                                                                 22,27
  20100
                                                                 23:00


                                                                 01136


                                                                  23:03
             20:00
                                  21100
                                                       22:00
                                                                            23100
                                                                              .H
                                              A4.46C.
                                              A5.34X.
.9.4X3

17.5X3

-5.6X3

.3. 8X3

.1. 9X3
                                                       .0. 0X0
                                                          Time
                                                                                     -2.9X5

                                                                                     .2.3X5

                                                                                     .1. 8X5

                                                                                     .1.2X5

                                                                                     .5.8X4
                                                        0.0X0
                                                           Tim.
                                                                                     -3.8X5

                                                                                     ~-3. 0X5

                                                                                     -2.3X5

                                                                                     .1.5X5

                                                                                     .7.6X4
                                                                                      0.0X0
                                                                                         Tim
                                                                                     _4.3E5

                                                                                     .3.4X5

                                                                                     '-2.6X5

                                                                                      .1. 7X5

                                                                                      .8.5X4

                                                                                      0.0X0
                                                                                            23,44
                                                       -1. 7X6

                                                       .1.4X6

                                                       Ll. OE6

                                                       .7.0X5

                                                       .3.5X5

                                                        0.0X0
                                                            Tim
                                                                                                         82

-------
rlleiS975866 #1-905 Acqil3-SEP-1997 Oli33i37 XI+ Voltage SIX 70S Hoimet5$
339.8597 7:2 BSDB(256, 30, -3. 0) PKD(7 ,5,3,0 .05\, 333.
TRIANGLE LABS TextiO-M23-l TLII43085
1004 A6.20E4
"'
60. |
:
40.

20. A3. 73X4 A9.01X3 M
o,i.oo\,r,T> XXPIXPCUS
ixr. TIMX - oii36
-3.3X4

1 > '•
! :
1
A3. 48X4 A4'.59X4 \ A1.07X4 '•
J\ ,^.«^jAJ *7'*S*\S.26X3\ It'-
o ^ /^V^ AJV JLAjl/yAA^A-, ^, f lA yVv^AA-fv 7V.A/ MAVviAJk— AJVYIA (V VA/l.AA. AlWAjta A /L A JITu A~A/<»'
24 > 00 25 : 00
2.6X4
2.0X4

.1 . 3X4

.6.6X3
0.0X0
26\00 \ 27 t 00 Time
FileiS975866 #1-905 Acgi 1J-MT-1997 Olt33t37 EI+ Voltage SIX 70S Hoim:63
341.8567 Ti2 BSUB(256, 30, -3.0) PXD(7,5, 3, 0. 05%, 252.
raXAMEV LABS Text:O-M23-l TLH43085
1001
eo:
60:
'• A9.70X4
«>-. A
20 \\
' I \A5.96X3 A1.06E4 j^4" A Al
rt ' jf V A -A. >^\jduA-» A A^. An~A - • mi «^ ^V- i^O'"*- * n n
24100 ' ' 25:00 '
0,1.00\,F,T) SxpiEPCUS \
IXT. TIMX - Oil 36
A1.89X5 ! -5.1X4


/


.46*4 , .V . *f.00*3 ,
^"^^*r**n ^* ^***L^ "^ A_*J \^^« A* * ™ ' A^A jiA _A^ AAA^ «j^
.4.1X4
.3.1X4

.2.1X4
.1 . 0X4

a .oso
2tf:00 27:00 Ti*e
rileiS975866 #1-905 Acqil3-SEP-1997 Olt33t37 EI+ Voltage SIX 70S Soiaet59
351.9000 T:2 BSUB(256, 30, -3.0) PKD(7 ,5,3,0. 05\, 236.
TRIANGLE LABS Text:O-M23-l TLI»43085
1001
80:
60:

40:
20:
0 - -T- i •
24:00 25:00
0,1.00\,F,T) ExptEPCUS
JJW. TTME " 01:36
A1.10X6 -4.815

|
A7.25E5
A

J l / \
.3 . 8E5
.2.9X5

.1 . 9X5
.9.6X4
a. oso
2ff>00 27:00 Tlae
rile:S975866 #1-905 Ac?»l 3-SEP-1997 01:33:37 EI+ Voltage SIX 70S NbiaetSS
353.8970 Tt2 BSVB(256, 30, -3. 0) PKD( 7,5, 3, 0. 05%,220
TRIANGLE LABS TextsO-M23-l TLHf43085
lOOi
sol
60:

40:
20:
o- ^ . . ^
24 1 00 	 25:00 '
.o,i.oo%,r,r; EXPIEPCUS
XKT. n>ffi - 01:Jff
A8.95E5 3.6X5


AS. 12X5
A
I
J V / \ n
.2.9X5
.2.2X5

.1.4X5
.7.2X4
O.OEO
'26:00 	 27ioO 	 MJIC
File,S975866 #1-905 Acq:13-SEP-1997 01:33:37 XI+ Voltage SIX 70S
330.9792 T:2 Exp-.EPCVS
TRIANGLE LABS TexttO-M23-l TLH43085
1004.
•
80:
go: 	 	 i ~ — 'X3iJ!>~
    00 25:00 JKT. TIMS - 01:35 27jlS—*-2X6 26:03 jUjJU—0^'/^ 7i* nT;iT^J\ J -2^52SS^^^ r f^ •J . 4X6 .2.5X6 .1 . 7X6 .8.4X5 O.OEO 26:00 27:00 Time rile:S975866 #1-905 Acq:13-SEP-1997 01:33:37 XI+ Voltage SIX 70S 409.7974 F:2 XxpiXPCUS TRIANGLE LABS TexttO-M23-l TLH43085 1003 HKT. TIME - 01:3ff 1 . 7Z4 801 25,35 60: 23:39 ^ 1 • R 25:lff 1 0: fy*^J\A^t\~rfU\J&^^^ 24 i 00 25:00 27:36 25.52 ^jM a5,jl- 27J21I 1 LA-jLuv^_Uj__Wl\^^^ -.1.3X4 .1 . 0X4 .6.7X3 .3.3X3 -'• o.oxo 26:00 27:00 Time 83

-------
355. J
TSIM
1001
80.
60.
40.
20.
S97TB6G 91-905 Ac2 faVB(256,30,-3.0) PXD(7,S,3,0.05\r232.0,1.00\rr,T) XxptXTCUS
tSLX LABS Text:0-K23-l TLH430S5 . IJW. TIM* • Oli36
A2.08X5 6.3X4
1
j\

A7.94E3 34 A3. 67X4 A1.06X4 *1-46s4j\ ^'l3" A1.88X4
~^J^fl^ *^f^S.^f. f^A. ^J^^J^^^-^f^JV \ VMyiJWLfA^lA. 	 ,-~r~. ^^.^AAAA
24:48 25:00 25:12 25:24 25:36 25:48 26:00 26:12 26:24 26:36 26:48 27:00 27:12 27:24 27:36
.5 . 0X4
.3 . 8X4
.2.5X4
.1.3X4
.o.oxo
Time
rile; 3975866 tl-905 Acqtl3-SXP-1997 01:33:37 EI+ Voltage SIS 70S SoimetS2
357.8516 Fi2 BSUB(256,30,-3 .0) PKD(7,5,3,0.05\r209.0,1.00\^r,T) ExpiEPCUS
TKIASSLX LABS T*xt:O-M23-l TLH43085 \ UKT. TIKE - Oil 36
1001
80.
60.
40.
20.
0'
2




Al 22E4 *2-laX4
4:48 25:00 25:12 25:24 25:36 25:48 26:00 26:12 26:24 26:36 26:48 27:00 27:12 27:24 27:36
.2.4X4
.1.9X4
.1.4X4
.9.SE3
'.4.8X3
'0.0X0
Time
Tile:S975866 tl-905 Acqil3-SEP-1997 01:33:37 EH- Voltage SIS 70S Soime:68
367.8949 F:2 BSVB(256,30,-3.0) PKD(7,5,3, 0. 05\,272. 0,1. 00%, T, T) ExptEPCUS
TRIANGLE LABS Tejtt : O-M23-1 TLI#43085 INJ. TIKE - 01:36
1001
so:
50:
40:
20:
0
A6.53E5




A7.85X4 I A,
r - r- i r - - -! i" TV - A - r . /\^ -, , - -r f - -, ^ V/^T
!4 : 48 ' 25:00 ' 25:12 25:24' 25:36' 25:48 26:00 ' 26:12 26:24 26:36' 26:48 27:0o' 27:12' 27:24 27: 36
.2.8X5
.2.2X5
.1 . 7X5
_1 . 1E5
.5.5E4
0 . OEO
Time
F±le:S975866 tl-905 Acq:13-SXP-1997 01:33:37 EH- Voltagre SIS 70S Koiae:47
369.8919 F:2 BSUB(256,30, -3.0) PKD(7,5,3, 0. 05%,188. 0,1. 00%,r, T) EipsEPCUS
TRIANGLE LABS Tert:O-J«23-l TLH43085 UKT. TIKE - 01:36
1003
80.
60.
40.
20.
0
A4 . 8X5



A1.13X5
A1.16X4 _A
1 /\ A2.19E4 1 A
^-Wrf - r 	 ^ T -f. ^^.,-A^A. ^^ A ^ VA ^r -t ri'S rt" ' ^VA
24:48 25:00 25:12 25:24 25:36 25:48 26:00 26:12 26:24 26:36 26:48 27:00 27;12 27:24 27:36
-1 . 6E5
11.3E5
.9.7X4
.6.5E4
.3.2X4
.0.0X0
Time
F±le:S975866 tl-905 Acqil3-SEP-1997 01:33:37 XI+ Voltage SIS 70S
330.9792 T>2 XxptXPCUS
TRIANGLE LABS TejcttO-H23-l TLIt43085 IKT. TIME - 01:36
100.
80.
60
40
20.
0
5
M ..„ /C, nn^/^V^^
25:01 25 ilS A?* lj\\ /** ^^ V
VVAA' ^
V
4.2X6
\'-
.3.4X6
.2.5X6
LI . 7X6
.8.4X5
0.0X0
24:48 25:00 25:12 25:24 25:36 25:48 26:00 26:12 26:24 26:36 26:48 27:00 27:12 27:24 27:36 Time
84

-------
rile: 5975866 tl-346 Aoq»13-SXP-1997 01:33:37 EH- Voltage SIX 703 Hoi*e:1094
373.8208 F:3 BSUB(256,30,-3 .0) HO>(7,5,3, 0.05\,4376 .0,1.00\,r,T) XxpiXTCUS
TRIANGLE LABS TmxttO-M23-l TLH43085 J1K7. TIMX " 01:36
1004
80:
60:
40:
20.
0:
rile
375.
TRIA
1001
801
601
40J
20.







A5i£?" J7.JU0" A2-52W
^^A>j\^^^_^_xMA(WVW^AJv^^^%^v^AvAA~^^
28:12 28:24 28:36 28:48 29:00 29:12 29:24 29:36 29:48 30:00 30:12 30:24 30:36 30:48 31:1
-.3975866 tl-346 Acqtl3-SXP-1997 01:33:37 XI* Voltage SIX 70S «oi»e:1144
8178 r:3 BSUB(256,30,-3.0) PKD(7 ,5,3 ,0 .OS\, 4576 .0,1 .00\,T,T) XxpiXPOJS
NGLE LABS TmxttO-M23-l TLH430B5 IJKT. TIMX - 01:36







42.42*4
-6.2*4
.4.924
-3.7X4
.2.5X4
.1.2X4
.0.0X0
10 Time
..1.915
11.5*5
.1.115
.7.4*4
L J . 7*4
       28:12 28:24  28:36 28:48  29:00 29:12  29:24  29:36 29:48  30:00 30:12  30:24 30:36
Tile:S97S866 tl-346 Acq:13-SEP-1997 01:33:37 El* Voltage SIB 70S JR>i*e:1149
383.8639 T:3 BSUB(256,30,-3.0) PKD(7,5,3,0.05\,4596.0,1.00\,T,T) ElptEPCUS
TRIANGLE LABS  Text:O-M23-l  TLIt43085                       ISJ. TIME -   01:36
1004                                                A4.98E5
                                                                                                   4.0.0*0
                                                                                                   : 00   Time
 80.;
 60:
 40:
 20:
                          A3.67E4
                                                                  A3.40*5
                                                                                        A2.45E5
.2.2*5
Ll. 7*5
-1. 3*5
.8.7*4
.4. 3*4
                                                                                                      0.0*0
       28:12  28:24 28:36  28:48  29:00 29:12  29:24 29:36  29:48 30:00  30:12 30:24  30:36 30:48 31:00   rifle
rile.-SS75865  #1-345 Acq:13-SEP-1997 01:33:37 EI+ Voltage SIR 70S Soiaetl283
385.8610 T:3  BSUB(256,30, -3. 0) PKD(7,5,3, 0. 05%, 5132. 0,1. 00%,r, T) Exp:EPCUS
TRIANGLE LABS  Text:0-M23-l TLH43085                       IWJ. TIME  -   01:36
1004                                               A9.79E5                                         _4.1*5
 80:
 60:
 40:
 20:
                                                                   A65
                                                                                        A4.70*5
L3.3*5
12.4*5
:i. 5*5
18.2*4
                                                                                                      0 . OEO
        28:12 28<24 28>J5  28:48 29:00  29:12 29:24  29:36 29:48 3ooO  30:12 30:24  30:35 30:48  31:00   Time
rile:S975866 tl-346 Acq:13-SEP-1997 01:33:37 EH- Voltage SZJZ 70S
392.9760 T:3 ExptEPCOS
TRIANGLE LABS  Text:O-M23-l  TLIt43085                       J7W. TIME -
100J
 80:
 60:
 40:
 20:
                                                                            01:35
                                                                                     30:36   30:50
 .4.1X6
 -3.2X6
 1.2.4X6
 .1.5*6
 .8.1*5
  0.0*0
        28:12 28:24  28:36 28:48  29:00 29:12  29:24 29:36 29:48  30:00 30:12  30:24 30:36  30:48 31:00
 rile.-S975866 4*1-346 Acq:13-SEP-1997 01:33:37 *!+• Voltage SIR 70S
 445.7555 Tt3 ExptEPCUS
 TRIANGLE LABS  TexttO-M23-l  TLH43085                       INJ. TIME -   01:36
                                                                                                          Time
 1003
  80:

  40:
  20:
   OJ
                     28i37
                            ....  .~                                                           30:46
                            a8>48     29,06                                   30,20           i

       A^fci^LJl^J
  2.2*4
 .1. 8*4
 .1.3*4
 .8.8*3
 14.4*3
                                                                                                      •o.oxo
        28: 12  28i24 28: 36  28:48 29: 00  29tl2 29: 24 29: 36  29: 4 8 3o:o   3012 3034  30:36 3o:48  3l:00   T±*»
                                                                                                         85

-------
 'Um:S975B6S il-346 Acq,13-3XP-1997 01,33,37 gH- Veltaga SIS 70S Hoi,.,1006
 89.8156 Ti3 BSUB(256,30, -3. 0) na>(7,5,3,0.05\,4024.0,1.00\,r,T) ExptfPCUS
TRIAHSLX LASS  T*xtiO-M23-l  TLH43085                       IXT. TIMS *   01>36
 001       A2.08E4
     28', 36   28:48   29s 00    29,12    29,24    29,36   29,48    30,00   30:12    30:24   30>35
 ile:S975866  tl-346 Acqtl3-SEP-1997 01,33t37 EH- Voltagre SIX  70S Soim*t964
 91.8127 Ts3  BSUB(256,30,-3.0) PXD(7,5,3,O.OS\,3856.0,1.00\,T,T) ExptEPCUS
TRIANGLE LABS  Text:0-K23-l TLH4308S                       IK7. TIME *    01:36
 001
     28:36   28,48    29:00   29:12    29,24   29,36    29,48   30,00    30,12   30,24    30,36
 rile:S975866 tl-346 Acq:13-SEP-1997  01:33,37 EH- Voltage SIX 70S No±ae:896
  01.8558 T,3 BSOB(256,30,-3.0) PKD(7,5,3,0.05\,3584.0,1.00\,r,T) EipiEPCUS
 TRIANGLE LABS  T&xt:O-M23-l TLH43085                        IK7. TIME -   01,36
  004                                                                     A6.55E5
  80.
  60.
  401
  201
                                                  Al.70X4

                                                        Al.79E4
                      A1.14E4
          Al.52E4
1.2E4


.1. OE4


.7.5E3


.5. OE3


.2.5E3
  80.

  60.

  40:

  20:
             A9.98E4
                        A2.52E4
                        .	A	^
                                                                                      A5.48E5
                                                                                                  O.OEO
                                                                                                     Tim,
                                                                                           2.7E5

                                                                                           2.2E5

                                                                                           .1. 6E5

                                                                                           .1. 1E5

                                                                                           .S.5E4
     28:36    28,48   29:00    29:12   29:24    29:36   29:48    30,00   30:12    30:24
  •ile,S975866 tl-346 Acq:13-SEP-1997 01,33:37 EI+ Voltage SIS 70S Hoite:799
 403.8529 F:3 BSUB(256,30,-3 .0)  PKD(7,5,3, 0. 051,3196. 0,1. 00%,T, T) Exp,EPCOS
 TRIANGLE LABS  Text:0-H23-l  TLI#4308S                       HKT. TIME  -   01:36
 1004                                                                      AS. 52E5

  ao:

  so:

  401
  20:
                                                                                          30:36
                                                                               A4.45E5
                                                                                                   O.OEO
                                                                                                      Tim
             A6.10E4
-2.3E5

'.1.9E5

-1.4E5

-9.3E4

.4. 6E4
      28,36   28,48    29,00   29:12    29,24   29:36    29,48   30:00   30,12    30,24
 r±le,S975866 tl-346 Acq,13-SEP-1997 01:33:37 EI+ Voltage SIR 70S
 392.9760  T:3 ExptEPCUS
 TRIANGLE  LABS  TexttO-M23-l TLI#43085                        IXJ.  TIME -   01,36

                                                                           30:14  30:24
   80.

   60.

   40.

   20'.

    0.
                                                                                          30,36
                                                                                   30:36
                                                                                                   O.OEO
                                                                                                      Tin
28:38
          28:52
                                       39:33 29:31  29,41 3*I49. 39,51
-3.7E6


.3.0E6

.2.2E6


L1.5Z5

.7.5X5
      28:36   28:48   29:00   29:12   29,24    29,36    29,48   30:00    30:12   30,24    30,36
                                                                                            O.OEO
                                                                                               Tim

-------
File,3975866 tl-390 Aoq:13-SEP-1997  01:33:37 Eli- Voltage SIX 70S Soiu»:»»0
407.7818 F:4 BSUB(356,30,-3.0) PKD(7,5,3,0.05\,353Q.O,1.00\,T,T) XxpiEtCUS
TRIANGLE LABS  Tmxt:0-H33-l TLIt43085                        1X7. TIME -   01:36
                    Al.76E4
     31:48      32'tOO     32', 12      32i24     33i36     32,48      33,00     33,12
F1101S975866  tl-390 Acq:13-SEP-1997 01:33:37 XI+ Voltage SIX 70S Holm*,889
409.7789 Ts4  BSU3(256,30, -3.0) PJO>(7,5,3, 0.05%,3556.0,1.00\,T,T) ExptEPCVS
TRIANGLE LABS  T*xt:O-M33-l TLIt43085                       IKT. TIME  -  01:36
1004
                                                                               33134
      31',48     32-00     32:12     32:24     32:36      32:48     33:00      33:12
 r±le,S975866 tl-390 Acq:13-SEP-1997 01:33:37 EI+ Voltage SIX  70S  Noise-.992
 417.8253 F:4 BSUB(256,30,-3.0) PKD(7,5,3,0.05\,3968.0,1.00\,T,T)  ExptEPCUS
 TRIANGLE LABS  T*xt:O-H23-l TLIt43085                       INJ.  TIKE -   01:36
 1001               A2.40E5
                                                                                         33:24
  80:

  601

  40:

  20:
      31:48     32,00      32:12     32:24      32:36     32:48      33:00      33:12
 rile:S975866 tl-390 Actj:13-SEP-1997 01:33:37 EI+ Voltage SIX 70S Noise1829
 419.8220 F:4 BSUB(256,30, -3. 0) PKD(7,5,3,0. 05%,3316.0,1. 00\,T,T) Exp:EPCVS
 TRIANGLE LABS  Text:O-M23-l  TLIt43085                        HKT. TIME -   01:36
                                                                     A1.48E5
                                    A5.48E4
                                                       A2.03E4
                                                                                     2.07E4
                                                                                          33:24
 1003
  ao:
  60:
  40:
  20:
                                       T
                                                                     33:00
     31li48'   '  32:00      32:12     32:24      32:36     32:48
F±le:S975866 tl-390 Acq:13-SEP-1997 01:33:37 EH- Voltage SIR 70S
430.9729 F,4 Eip-.EPCDS
TRIANGLE LABS   Tsxt:O-M23-l  TLIt43085                       rVJ. TIME »
                    AS. 63E5
                                                                      A3.39E5
                    -f
                                                                               33,12
                                                                                          33:24
                                                                             01:36
  1003
   sol
   60:
   40:
   20!
                                                                     33:00
       31:48     32:00      32:12     32:24     33:36      32:48
  r±le:S975866 tl-390 Acq:13-SEP-1997 01:33:37 EH- Voltage SIR 70S
  479.7165 F:4 EipiEPCUS
  TRIANGLE LABS  Text:0-M33-l TLIt43085                        ISJ. TIME -   01:35
31:5231:58^32:06
                  32:13  32:21  32:28
                                                                                33:12
                                                                                          33:24
                                                                                                     1. OE5

                                                                                                     8.3E4

                                                                                                     6.2E4

                                                                                                     .4.1E4

                                                                                                     .2.1E4

                                                                                                     .O.OEO
                                                                                                         Tiae



                                                                                                     .2.4ES

                                                                                                     .1.9E5

                                                                                                     .1.4E5

                                                                                                     9.4E4

                                                                                                     4.7E4
                                                                                             O.OEO
                                                                                                Time
                                                                                                      3.4E6

                                                                                                     .2.7E6

                                                                                                     .2.1E6

                                                                                                     .1.4E6

                                                                                                     .6.8E5
                                                                                                       .O.OEO
                                                                                                           rifle
                                                                                                           87

-------
 'ile:SS75BSS tl-390 Aotj:13-stt-19S7 01:33:37 K+ Voltage 3H 703 Boi»«.5fl7	
 23.7766 ri4 SSVS(3S6,30, -3.0)  PXD(7,5,3,0.05\,2348.0,1.00\, f,T) XxptXTCOS
TXIAHGLX LASS  Tejft,O-M23-l  TUH3085                       OKT. TIM* -   Oil 36
 00\                           A3. f 3X4
   33', 00   33', 06   32:12  32:18   32',24  32:30  32',36   32:42  32:48  32:54
 ±le:S975866  91-390 Acq:13-SEP-1997 01:33:37 XI* Voltage SIX  70S Nairn*-.533
 25.7737 T:4  BSUB(256,30,-3.0) PXD(7,5,3,0.05\,2132.0,1.00\,r,T) XxptEPCUS
TRIANGLE LASS Text:0-M23-l TLH430BS                       IKT. TIKE -  01:36
  001                           A3.38E4
                                                                  33\00 ' '33',06
33:12
   32:00   32:06  32:12   32-.18  32:24  32:30   32:36  32:42  32:48   32:54  33:00   33:06
 FileiS975866 H-390 Acq:13-SEP-1997  01:33:37 EH- Voltage SIX 70S Noiae:590
  35.8169 T:4 BSV3(256, 30, -3. 0) PKD(7, 5,3 ,0 .OS\,2360 .0,1,00\,T,T) Exp:EPCUS
 TRIANGLE LASS  TfXt:O-H23-l TLH43085                        IKJ. TIKE "   01:36
 1004                                                              A3.61ES

  SOJ

  so:

  40:

  20J
                                                                                                  0.0EO
                                                                                            33:12    Time
                                                                                       1.5ES

                                                                                      '.1.2E5

                                                                                      .9. 2E4

                                                                                      .6.1S4

                                                                                      .3.1E4
                                                                                                 .O.OEO
    32:00  32:06   32:12  32:18  32:24   32':30  32:36  32:42   32:48  32:54   33:00   33:06  33:12    Time
 rile:S975866 #1-390 Acq:13-SEP-1997 01:33:37 EI+ Voltage SIX 70S Ooiae:220
 437.8140 F:4 SSU3(256,30,-3.0)  PKD(7,5,3,0.OS\, 880.0,1.00\,F,T) Exp:EPCUS
 TRIANGLE LASS  Text:O-M23-l  TLKM3085                       JK7. TIKE -   01:36
 1004                                                              A3.56E5
  so:

  60.

  40.

  202
                              A3.68E4
                                                                                      -1.4ES

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                                                                                      .8.2E4

                                                                                      -5.5E4

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                                                                                                  .O.OEO
    32:00   32:06  32,12  32:18   32:24  32:30  32:36   32:42  32:48   32:54   33:00  33:06   33:12
                                                                                                      Time
 rile:S975866 tl-390 Acq:13-SEP-1997 01:33:37 EI+ Voltage SIX  70S
 430.9729  F:4 ExpiEPCUS
 TRIANGLE  LASS  TeJCt:O-M23-l TLH43085                       JJK7.  TIME -
                                                                             01,36
  1001

   80.

   60.

   40.

   20.

    0.
32:06
         32:13
                   32:21
                            32:28
      ^3.4X6

      '.2.7X6

      12.0X6

      1.1.4X6

      .6.8X5
                                                                                                  .0.0X0
    32:00   32:06  32:12   32:18  32:24  32:JO   32:36  32:42   32:48   32:54  33:00  33:06  33:12
                                                                                                      Time

-------

-------
 'H0.3S7SBSS 11-390 Aog:13-SXP-19!>7 01,33,37 fH- Voitag* SIS 70S Hoi*.,335	
 57.7377 T,4 BSWS(256,30,-3.0)  PKD(7,5,3,0.05\,900.0,1.00\,r,T) XzptfPCOS
TRIANGLE LABS  T*JCt,O-M23-l  TLH43085                       IJKT. TIM* -   Oli36
                                                                                   35,42
             35,12         35,18         35,24         35,30         35:36
 ila:S975866 tl-390 Acq,13-SEP-1997 01,33,37 XI* Voltagw  9IX 70S Nairn*,359
 59.7348 r,4 BSUB(256, 30, -3. 0) PXD(7,5,3, 0. 05\,1436. 0,1. 00\,r,T) ExptEPCOS
TRIANGLE LABS   Text:O-M23-l  TLIt43085                        IHJ. TIME -   01,36
  004
  801
  50.
  401
  201
             35:12         35:18         35:24         35:30         35:36         35:42
.FileiS975856 #1-390 Ac
-------

-------
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115.9419 F:2 Exp.-EPCUS
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-------
'ile:S975866  #1-905  Acq:l3-SEP-1997 01:33:37 EI+ Voltage SIR 70S
119.8965  F:2  Exp:EPCUS
Jample Text:O-M23-l  TLI#43085                       INJ. TIME =   01:36  File  Text:O-M23-l  TLI#4>
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           20:00         21:00        22:00         23:00        24:00
'ile:S975866  #1-905 Acq:13-SEP-1997 01:33:37 EI+ Voltage SIR 70S
21.8936  F:2  Exp:EPCUS
Jample  Text:O-M23-l TLI#43085                       INJ. TIME =   01:36 File  Text :0-M23-J. TLI#4»
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'ile:S975866 #1-905 Acq:13-SEP-1997  01:33:37  EI+  Voltage SIR 70S
31.9368 F:2 Exp:EPCUS
lample Text:O-M23-l TLI#43085                       INJ.  TIME =    01:36 File Text:0-M23-l TLI#4»
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-------
'ile:S975866 #1-905 Acq: 13-SEP-1997 01:33:37 EH- Voltage SIR 70S
51.9000 F:2 ExprEPCUS
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53.8970 F:2 Exp:EPCUS
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-------
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23.7766 F:4 Exp.-EPCUS
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-------
TLI Project:      43085
Client Sample:   O-M23-2
Method 23 PCDD/PCDF Analysis (a)
             Analysis File:   S975867
Client Project:
Sample Matrix:
TLI ID:

Sample Size:
Dry Weight:
GC Column:
S413-004
M23Train
181-55-2ABE

1.000
n/a
DB-5

Date Received:
Date Extracted:
Date Analyzed:
Dilution Factor:
Blank File:
Analyst:

09/03/97
09/04/97
09/13/97
n/a
S975815
ML

Spike File:
ICal:
ConCal:
% Moisture:
% Lipid:
% Solids:

SPX23704
SF56117
S975861
n/a
n/a
n/a
Analytes • '•".• "">... i-\J'. •.'>':
2,3,7,8-TCDD
1,2,3.7,8-PeCDD
1,2,3,4,7,8-HxCDD
1,2,3,6,7,8-HxCDD
1,2,3,7,8,9-HxCDD
1,2,3,4.6,7,8-HpCDD
1,2,3,4,6,7,8,9-OCDD
2,3,7,8-TCDF
1,2,3,7,8-PeCDF
2,3,4,7,8-PeCDF
1,2,3,4,7,8-HxCDF
1,2,3,6,7,8-HxCDF
2,3,4,6,7,8-HxCDF
: -2,3,7,8,9-HxCDF
1,2,3,4,6,7,8-HpCDF
1,2,3,4,7,8,9-HpCDF
1,2,3,4,6,7,8,9-OCDF
Totals
Total TCDD
Total PeCDD
Total HxCDD
Total HpCDD
Total TCDF
Total PeCDF
Total HxCDF
Total HpCDF
:••" :; Amt: (ng)
ND
ND
ND
i~i-/
ND
ND
ND
ND
ND
EMPC
ND
ND
ND
ND
FMPC
LJlVti V_^
ND
ND
ND
Amt (ng)
ND
EMPC
0.44
EMPC
ND
EMPC
EMPC
EMPC
Dt EMPP.:':!^^
0.07
0.09
n i
U.I
0.1
0.1
0.2
0.6
0.05
0.24 E
0.07
0.09
0.07
0.08 	
n 94. /"\c
0.2 " ~
0.2
0.4 ~
:' Numbef;:' DL : -EMPC'' '••'^^:T<^-^''-r^^:f^;^'^-'f^.j^g^/;:
0.07
1.0 

SR vZOO. LMS6.10M Triangle Laboratories, Inc.® 801 Caprtola Drive • Durham, North Carolina 27713 Phone: (919) 544-5729 • Fax: (919) 544-5491 Printed: 12:07 09/1


-------
TLI Project:      43085
Client Sample:   O-M23-2
Method 23 PCDD/PCDF Analysis (a)
             Analysis File:   S975867
Internal Standards
13C,2-2,3,7,8-TCDF
13Cn.-2,3,7,8-TCDD
13C12-l,2,3,7,8-PeCDF
13C,:-l,2,3,7,8-PeCDD
13C,:-l,2,3,6,7,8-HxCDF
13C,2-l,2,3,6,7,8-HxCDD
13Cp-l,2,3,4,6,7,8-HpCDF
I3C,rl,2,3,4,6,7,8-HpCDD
13C12-1,2,3,4,6,7,8,9-OCDD
Surrogate Standards (Type A)
37CL-2,3,7,8-TCDD
13C,:-2.3,4,7,8-PeCDF
13Cp-l,2.3.4,7,8-HxCDF
13Cp-l,2,3,4,7,8-HxCDD
IJC,:-l,2,3,4,7,8,9-HpCDF
Alternate Standards (Type A}

13Cp-l,2,3,7,8,9-HxCDF
13C,2-2,3,4,6,7,8-HxCDF
Recovery Standards :-:£: ^1^
13C12-1,2,3,4-TCDD
13C,2-l,2,3,7,8,9-HxCDD
Arrrt. {ng)
3.5
3.6
3.3
4.1
3.2
3.1
1.9
2.1
2.4
AmL (ng)
4.0
3.7
3.8
3.4
4.6
Amt. (ng) :

2.3
2.9
••'?•"'?' ••••:/:';::-:-.y:-.: •''••/-:

% Recovery
88.1
90.2
82.1
102
81.0
77.6
47.2
53.2
29.8
; " ^ Recovery
100
93.1
943
85.6
116
' '• '•• -•• :-:"%' Recovery

58.2
73.7
^™^V|:S-?»V

QC Limits
40%- 1 30%
40%- 130%
40%- 130%
40%- 130%
40%- 1 30%
40%- 130%
25%-130%
25%- 130%
25%- 130%
QC Limits
70%- 140%
70%- 140%
70%- 140%
70%- 140%
70%- 140%
QC Limits

40%- 130%
40%- 130%
•^f^^/;::

Ratio
0.77
0.83
1.11
1.44
0.52
1.36
047
1.11
1.00
Ratio
1.33
056
1 31
0.42
•!•••••• Ratia--^"

055
0.47
^t^Raiio-SI
0.84
1.20
RT
23:16
23:47
26:29
27:23
29:37
30:15
32-05
32:52
35:22
•^P>*
23:47
27:06
29-33
30-11
33:13
^'"'".RT "

30-44
30:04
•li%«ri:;
23:36
30:31
Ftegs
OH
Q_
o
Q
Q 	
•:''7yiFtagsV;;-
0
n
Q_
Flags

n
Q 	
^ifiagsf;
Q—
                      Data Reviewer.
                                         Page 2 of 2
              09/18/97
                            X237.PSR vZOO. UkRSfcK
 Triangle Laboratories, Inc.®
 801 CapHola Drive • Durham, North Carolina 27713
 Phone: (919) 544-5729 • Fax: (919) 544-5491
                        Panted: 12:07 09/18/2
                                   , I S

-------
                                 ...Date...
Data Review By:
                                            Calculated Noise Area:
The Total Area for each peak with an ion abundance ratio outside
ratio limits has been recalculated according to method requirements.
                                                                    1.02
Page No.
09/18/97
Listing  o£ S975867B.db£
Matched  GC Peaks / Ratio /  Ret. Time
Compound/
M_Z....  QC.Log Omit Why ..RT.  OK Ratio Total.Area...  Area.Peak.1..  Area.Peak.2. .  Rel.RT  Compound.Name..  ID..  Flags.
TCDF
304-306










304-306
13C12-TCDF
316-313






316-313
TCDD
320-322
















0.65-0.89
DC
DC
DC
DC
DC
DC
DC
DC
DC
DC
DC


DC
DC
DC
DC
DC
DC



DC
DC
DC
DC
DC
DC
DC
DC
DC
DC
DC
DC
DC
DC
DC
DC
DC
NL
ML
WL
SN
SN
SN
SN
SN
SN
SN
SN
0

NL
WL
WL
WL
WL
SN

1

NL
WL
WL
WL
WL
WL
WL
SN
SN
SN
SN
SN
SN
SN
SN
SN
SN
0:
18:
19:
19:
20:
21:
22:
22:
22:
22:
22:
00
27
27
43
41
20
00
14
25
37
50
RO
RO
RO
RO
RO
RO



RO

1.
1.
2.
3.
4.
1.
0.
0.
0.
2.
0.
27
03
47
15
86
15
73
69
si
14
37
Peaks

0:
18:

00
27
19:26
20:
03
20:15
22:
23
:21
:16
0.
RO
RO
RO
RO
RO
RO

0.
0.
2.
2.
0.
3.
5.
1.
3.
1.
2.
0.
19
57
37
76
39
59
04
49
90
13
21
00
65-0.89
1.
0.
1.
0.
24
24
46
33
1.16
2.84
0.
Peak

0
19
19
20
20
20
20
21
21
21
21
21
22
22
22
22
23

:00
:23
:43
:10
:22
:29
:38
:07
:13
:25
:46
:54
:03
:15
:34
:43
:29
0.

RO
RO
RO

RO
RO
RO
RO
RO
RO
RO
RO
RO

RO
RO
.77

65-0.89
0
2
0
0
0
0
1
1
0
0
1
1
0
1
0
2
1
.75
.27
.61
.48
.65
.27
.35
.84
.54
.94
.22
.49
.56
.53
.84
.00
.38
0.
0.
0.
0.
1.
0.
154,
37
37
96
32
22
.65
.49 67.28
0.838-
0.
0.
0.
0.
0.
0.
0.
0.
0.
0.
0.

1.092
000
793
836
347
889
917
946
956
963
972
981

0.954-1.046
0.
0.
0.
0.
0.
0.
87.21 1.
000
793
335
362
870
.961
.000 13C12-2378-TCDF ISO
154.49

0
0
1
0
1
0
0
0
1
1
0
0
0
0
0
0
.35
.39
.24
.87
.17
.48
.87
.34
.03
.72
.41
.83
.85
.27
.57
.51
0.65
0.875-1.055
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
.000
.819
.829
.348
.856
.861
.868
.888
.892
.900
.915
.921
.927
.936
.949
.955
.987
Triangle Laboratories, Inc.® Analytical Services Division
801 Capitola Drive • Durham, North Carolina 27713
Phone: (919) 544-5729 • Fax: (919) 544-5491
                                                                     Printed: 12:01 09/18/97-
                                                                                  98

-------
  Page No.
  09/18/97
Listing of S975867B.dbf
Matched (X Peaks /  Ratio / Ret. Time
  Compound/

  M_2.... QC.Los Omit Why ..RT. OK Ratio Total.Area... Ar.a.P.ak.1.. Ar.a.Peak.2.. Rel.RT Compound.Name..  ID.. Fla,s.
DC
320-322
37C1-TCDD
328 DC
DC
DC
DC
DC
DC
DC
DC
DC
DC
DC
DC
DC
DC
DC
DC
DC
DC
DC
DC
DC
DC
DC
DC
328
13C12-TCDD
332-334 DC
DC
DC
DC
DC
DC
DC
DC
DC
DC
DC
DC
DC
DC
332-334
SN
0
NL
WL
ML
WL
WL
WL
WL
WL
WL
WL
WL
WL
WL
SN
SN
SN
SN
SN
SN
SN
SN
SN
SN
SN
2
NL
WL
WL
WL
WL
WL
SN
SN
SN
SN
SN
SN
SN
SN
2
23:40
Peaks
0:00
19:42
19:57
20:00
20:09
20:09
20:24
20:27
20:36
20:54
21:02
21:18
21:29
21:43
21:53
22:01
22:16
22:27
22: 34
22:41
22:52
23:05
23:19
23:27
23:39
23:47
Peaks
0
19
20
20
20
21
21
21
22
22
22
22
23
23:
:00
:39
:06
:18
:35
:09
:40
:52
:00
:12
:21
:50
:12
:25
RO
0.
RO
RO
RO
RO
RO
RO
RO
RO
RO
RO
RO
RO
RO
RO
23:36
23:47
Peaks
1
65-
3
1,
1,
11.
2
1.
4.
1
4
1
5.
0
0,
1,
0,
0,
.92
-0.89
.54
.87
.35
.75
.04
.50
,19
.44
.26
.42
.47
.46
.55
.41
.84
.83
1
0
0
9
0
0
0
0
0
0
0
0
0
0
0
1
0
0
1
1
0
0
0
0
0
0
12
108
120
0
6
0
0
0
0
0
0
0
0
0
1
1
2
132
127
260
.40
.00
.16
.29
.33
.10
.17
.20
.21
.30
.66
.64
.15
.47
.88
.09
.51
.31
.04
.15
.26
.71
.49
.51
.13
.49
.85
.07
.92
.23
.48
.35
.14
.87
.25
.64
.96
.67
.64
.27
.52
.08
.21
.99
.81
.80
0.995
0.910-1.090
0.000
0.828
0.839
0.841
0.847
0.347
0.858
0.860
0.866
0.879
0.884
0.896
0.903
0. 913
0.920
0.926
0.936
0.944
0. 949
0.954
0.961
0.971
0. 980
0.986
12.85 0.994
108 -07 1.000 37C1-TCDD SUR1
0.910-1.090
o. ooo
0.
0.
0.
0.
0.
0.
0.
0.
0.
0.
0.
0.
0.
SO. 76 72.23 0.
57.91 69.90 1.
826
845
854
865
389
911
919
.925
933
940
960
975
.985
992 13C12-1234-TCDD RSI
000 13C12-2378-TCDD IS1
Triangle Laboratories, Inc.®  Analytical Services Division
801 Capitola Drive • Durham, North Carolina 27713
Phone: (919) 544-5729 • Fax: (919) 544-5491
                                                                 Printed 12:01 09/18/9'
                                                                                   Q<

-------
Page No.
09/18/97
Listing of S975867B.dbf
Matched GC Peaks  / Ratio / Ret. Tin
Compound/
M_Z.... QC.Log Omit Why  ..RT. OK Ratio Total.Area...  Area.Peak.1.. Area.Peak.2.. Rel.RT Compound.Name..  ID.. Flags.
PeCDF
340-342


E



E


340-342
13C12-PeCDF
352-354




N
N
352-354
PeCDD
356-353









356-358
13C12-PeCDD
368-370





DC
DC
DC
DC

DC
DC
DC
DC
DC
DC
DC


DC

DC
DC
DC
DC
DC



DC
DC
DC
DC
DC
DC
DC

DC
DC


DC
DC
DC
DC

DC
NL
WL
WL
WL
(§y
SN
SN
SN
SN
\E..
SN
SN
SN
2

NL

SN
SN
SN
SN
SN

3

NL
WL
WL
WL
SN
SN
SN

SN
SN
1

NL
SN
SN
SN

SN
0:
23:
23:
24:
24:
25:
25:
26:
26:
26:
27:
27:
27:
00
29
40
30
53
20
55
08
1.32-1.78
RO 1.00
RO 0.89
RO
RO .
RO
RO
RO
RO
21 RO
32@
02 RO
27
45
RO
RO
0.
0.
1.
0.
0.
2.
9.
0.
0.
3.
4.
23
61
40
18
78
72
48
17
70
78
40
Peaks

0:
23:
24:
25:
26:

00
39
58
26
04
1.
RO
RO
RO
RO
RO
26:12
26:29(RO;
26:57
27:
:06

TULfU
0.
0.
8.
0.
5.
0.
1.
1.
0.
8.
0.
1.
3.
14.
16
66
01
44
86 3.56
53
09
63
79
29 5.04
94
02
09
15
32-1.78
1.
0.
7 .
0.
1.
20
68
83
48
21
1.70
1.11
1.37
1.
Peaks

0
24
25
25
25
25
26
26
26
27

:00
:48
:09
:27
:39
:50
:14
:30
:47
:36
1.
RO
RO
RO
RO

RO
RO
RO
RO
RO
.33

32-1.78
1
2
1
1
1
0
2
3
0
0
.09
.13
.26
.09
.51
.72
.07
. 05
.78
.33
Peak

0
25
25
26
26
26

:00
:12
:23
:10
:30
:59
1
RO
RO

RO
RO
RO
0.
9.
0.
20
92 6.03
61
0.44
1.
.63
2.13
123.77 75.23
5.93
111
245
PeCDl
0
0
0
0
1
0
1
27
0
0
27
.72 63.86
.41

.20
.20
.72
.41
.43
.46
.05
.95 33.38
.69
.58
.95
.32-1.78
0
0
1
0
0
0
.92
.40
. 57
.38
.44
.62
0
0
0
0
14
.18
.56
.95
.58
.99 9.11
0.64
0.915-1.074
0.000
0.867
0.
0.
2.54 0.
0.
0.
0.
0.
29.97 0.
0.
1.
1.

0.844-
0.
8.92 0.
0.
0.
0.
0.
67.88 0.
0.
47.86 1.

873
904
918
935
956
964
972
979 12378-PeCDF AN (Q ^
998
013
024

1.156
000
873
921
938
962
967
977 13C12-PeCDF 123 IS2 p
994 **-•"
000 13C12-PeCDF 234 SUR2

0.926-1.024
0.
0.
0
0
0
0
0
10.96 0
0
1

.000
. 902_
.915
.925
.933
.939
.954
.964 (Q]
.974
.004

0.850-1.150
0
0
0
0
20.64 0
0
.000
.916
.923
.952
.964
.981
Triangle Laboratories, Inc.® Analytical Services Division
801 Caprtola Drive • Durham, North Carolina 27713
Phone: (919) 544-5729 • Fax: (919) 544-5491
                                                                 Printed: 12:01 09/18/97
                                                                                »100

-------
  Page No.
  09/18/97
Listing of S975867B.«Jbf
Matched GC Peaks / Ratio  / Ret. Time
  Compound/
  M_Z.... QC.Log Omit Why ..RT. OK Ratio Total.Area...
                                                     Area.Peak.l.. Area.Peak.2..  Rel.RT Compound.Name..  ID.. Flags.
         N
         N
  368-370
 HxCDF
 374-376
         EK
 374-376

 isc12-HXCDF
 384-386
         N
         N
         N

         N
         N
 384-386
DC
DC

DC
DC
DC

DC
DC
DC
DC
DC
DC
DC
DC
DC
DC
DC
DC
DC
DC

DC


DC
DC
DC
DC
DC

DC
DC
DC
DC



DC
DC
SN
SN
3

NL
WL
WL
\§'
SN
SN
SN
SN
SN
SN
SN
SN
SN
SN
SN
SN
SN
en
0
SN
2

NL
SN
SN
SN
SN

SN
SN
SN
SN



SN
SN
27:08
27:23
27:30
27:41
Peaks

0:
28:
28:
28:
29:
29:
29:
29:
29:
29:
29:
29:
29:
30:
30:
30:
30:
30:
30:
30:

00
33
41
49
03
09
21
32
35
45
49
53
58
06
11
24
33
37
44
57
RO
RO
1.
RO

RO
RO
RO
RO
RO
RO
RO
RO
RO
RO


RO
RO
RO
RO
£0)
RO
1,
1
1
0.
.00
.44
.56
.52
,05-1.43
1,
1,
0,
1,
0,
2.
0.
1,
0.
0.
1.
3.
1
1.
0,
0.
0.
0.
0.
0,
.02
.35
.25
.40
,57
.03
,49
,80
.39
.62
.79
.50
.20
, 15
.56
,37
.45
,75
.89
.05
Peaks

0:
28:
28:
28:
28:
28:
23:
28:
29:
29:
29:
29:
30:
30:
30:

00
18
25
29
35
49
54
58
13
16
33
37
04
11
33
0.
RO
RO
RO
RO
RO
RO

RO
RO
RO



RO
RO
30:44
DC

SN
5
30:
55
RO
43-0.59
0.
0.
3,
0.
0
0
0.
0
1.
4,
0
0.
0.
0
1
0,
1
.94
.70
.46
.19
.39
.79
.54
.36
.13
.36
. 56
.52
.47
.82
.68
.55
.56
Peaks
  0.67
 86.32
 10.69
  0.23
112.00
                       1.81
                       1.48
                       0.13
                       6.97
                       0.47
                       0.65
                       0.45
                       1.10
                       0.45
                       1.28
                       0.94
                       1.03
                       1.23
                       3.09
                       1.63
                       0.70
                       1.32
                       1.32
                       6.63
                       0.20
                      13.60
  1.01
  0.69
  0.20
  0.50
  0.80
  9.44
  1.05
  0.63
  0.47
  0.17
 89.18
 98.61
 83.08
  1.10
  1.45
 57.08
  0.83
337.39
                                   50.92
                                    6.52
                                                          Follows
       0.987
35.40  0.996 13C12-PeCDD 123  IS3
 4.17  1.000
       1.007
                                                             4.35
                                                             3.67
                                                                                                      AN
                                                                                                      AN
                                                        AN
                                                        AN
                                                             4.91
                                   32.02
                                   33.78
                                   26.72
                                                            20.26
   0.959-1.050
       0.000
       0.950
       0.954
 3.11  0.958
       0.966
       0.970
       0.976
       0.982
       0.984
       0. 989
       0.992
       0. 994
       0.997 123478-HxCDF
       1.001 123678-HxCDF
       1.004
       1.011
       1.016
       1.018 234678-HxCDF
 4.12  1.022 123789-HxCDF
       1.029
   0.863-1.137
       0.000
       0.941
       0.945
       0.947
       0.951
 6.25  0.958
       0.961
       0.963
       0.972
       0.973
57.16  0.983 13C12-HXCDF 478 SUR3<
64.83  0.985 13C12-HxCDF 678 IS4
56.36  1.000 13C12-HXCDF 234 ALT2 <
       1.004
       1.016
36.82  1.022 13C12-HXCDF 789 ALT1|
       1.028
Triangle Laboratories, Inc.® Analytical Services Division
801 Capitola Drive • Durham, North Carolina 27713
Phone: (919) 544-5729 • Fax: (919) 544-5491
                                                                     Printed: 12J>1 09/18/S
                                                                                                        101

-------
 Page No.
 09/18/97
Listing of  S975867B.dbf
Matched GC  Peaks / Ratio / Rat.  Time
 Compound/
 M_Z	  QC.Log Omit Why ..RT.  OK  Ratio Total.Area... Area.Peak.1..  Area.Peak.2.. Rel.RT Compound.Name.. ID.. Flags.
HxCDD
390-392

K















D
390-392
13C12-HXCDD
402-404






N
N
N

402-404
HpCDF
408-410



408-410

DC
DC

DC
DC
DC
DC
DC
DC
DC
DC
DC
DC
DC
DC
DC
DC
DC
DC


DC
DC
DC
DC
DC
DC
DC






DC

DC
DC


NL
WL

WL
SN
SN
SN
SN
SN
SN
SN
SN
SN
SN
SN
SN
SN
SN
WH
1

NL
WL
WL
WL
WL
WL
SN




4

NL

SN
SN
1

0:
28:
28:
28:
29:
29:
29:
29:
29:
29:
29:
29:
29:
30:
30:
30:
30:
30:
30:

00
39
48
54
09
16
20
29
34
36
44
47
53
02
10
12
18
36
45
1.
RO
RO

RO


RO
RO
RO
RO



RO
RO
RO
RO
RO

	 ADOVe: HXCDF
05-1.43
0.
0.
1.
0.
1.
1.
0.
0.
0.
0.
1.
1.
1.
2.
0,
0,
1,
0.
1
83
35
34
86
14
23
53
23
25
63
,07
32
.23
.87
,59
.14
.88
.75
. 19
Peak

0:
28:
28:
29:
29:
29:
29:
30:
30:
30:
30:

00
40
49
11
15
20
32
11
15
31
43
1.
RO
RO
RO
RO
RO
RO
RO



RO
0.
0.
9.
1.
1.
1.
0.
0.
0.
0.
0.
0.
0.
0.
1.
0.
0.
1.
10.
9.
/ HXCDD Follows 	
99
13
02 5.17
19
50
05
89
33
14
47
91
95
78
69
05
20
58
28
16
02
05-1.43
0
2
2
0
2
5
2
1
1
1
1
Peaks

0:
32:
32:
33:

00
23
40
05
0,
RO
RO

RO
.87
.93
.23
.33
.25
.43
.78
.31
.36
.20
.85

,88-1.20
1
1
1
1
. 67
.79
.13
.77
Peak
1.
1.
16.
1.
0.
0.
0.
65.
78.
101.
18.
39
03
89
03
63
52
20
09 36.92
12 45.06
17 55.23
91 15.60
0.953-
0.
0.
3.85 0.
0.
0.
0.
0.
0.
0.
0.
0.
0.
0.
0.
0.
0.
0.
1.
1.

0.967-
0.
0.
0.
0.
0.
0.
0.
28.17 0.
33.06 0.
45.94 1.
8.44 1.
1.014
000
939
944
947
955
959
961
966
969
970
974
976
979
984
989
990
993
003
008

1.033
000
939
944
956
958
961
968
989 13C12-HXCDD 478 SUR
991 13C12-HXCDD 678 IS5
000 13C12-HXCDD 789 RS2
007
263.29

1.
5.
0.
2.
5.
.98
22 4.59
96
.18
.22
0.995-1.042
0.
2.56 1.
1.
1 .

000
009
018
031

 13C12-HPCDF                   0.37-0.51
 418-420         DC  NL   0:00 RO  1.24
                 DC  SN  31:58 RO  2.80
                        32:05     0.47
                        32:23 RO  1.43
                       1.48
                       0.66
                     42.38
                       8.57
13.48
 8.53
   0.937-1.125
       0.000
       0.996
28.90  1.000 13C12-HpCDF 678  IS6
 5.95  1.009
Triangle Laboratories, Inc.®  Analytical Services Division
801 Caprtola Drive • Durham, North Carolina 27713
Phone: (919) 544-5729 • Fax: (919) 544-5491
                                                                    Printed: 12:01 0!

-------
Page No.
09/13/97
Listing of  S975867B.dbf
Matched GC  Peaks  /  Ratio  / R«t. Tin
Compound/
M_Z.... QC.Log Omit  Why  ..RT. OK Ratio Total.Area...  Area.Peak.1.. Area.Peak.2..  Rel.RT Conpound.Nam*. .  ID.,
                                                                                  Flags.
418-420
 HpCDD
 424-426
 424-426

 13C12-HpCDD
 436-438
 436-438
 OCDF
 442-444
  442-444

  OCDD
  458-460
  458-460

  13C12-OCDD
  470-472

  470-472
DC
DC
DC
SN
SN
SN
3
32:41 RO
32:52 RO
33:13
33:31 RO
Peaks
0.63
0.65
0.42
0.57
0.88-1.20
DC
NL
0:00
32:22 RO
DC

WH
1
33:08 RO
0.95
0.64
0.45
Peak
0.88-1.20
DC
DC
DC
DC

DC


DC
DC

DC
DC
DC

DC
DC
DC
DC
DC
NL
SN
SN
SN

SN
1

NL
SN

SN
SN
SN

SN
SN
SN
SN
SN
0:
32:
32:
32:
32:
33:
00
02
11
22
52
14
RO
RO
RO
RO

RO
2.38
0.24
1.75
1.38
1.11
3.10
Peak

0:

;00
32:02
32
32
33
33
33
34
35
35
35
35
:22
:56
:09
:14
:53
:44
:03
:09
:26
:32
0.
RO
RO
RO
RO
RO
RO
RO
RO
RO

RO
RO
76-1.02
0.65
0.61
0.41
2.19
0.21
1.67
0.38
1.67
0.43
0.89
0.42
2.19
2 Peaks
               0.76-1.02
DC  NL   0:00  RO  1.38
      0 Peaks

               0.76-1.02
DC  NL   0:00     0.93
        35:22     1.00
      1 Peak
                                               0.66
                                               2.43
                                              37.78
                                               1.27
                                              88.73
                       1.21
                      11.35
                       1.53
                      11.85
                       0.59
                       0.31
                       1.45
                       2.98
                       43.39
                       1.06
                       43.39
                                    11.15
                                                          Follows
                                                             6.04
                                                              1.019
                                                              1.024
                                                       26.63  1.035 13C12-HpCDF 789 SUR5  Q
                                                              1.045
                                                             23.07
                                                          0.977-1.005
                                                              0.000
                                                         9.37  0.985
                                                              1.008
                                                           0.969-1.031
                                                               0.000
                                                               0.975
                                                               0.979
                                                               0.985
                                                        20.82  1.000  13C12-HpCDD  678  IS7
                                                               1.011
                                             HpCDD /  Octa-CDD and CDF Follows
                        1.40
                        1.17
                       11.70
                        0.51
                        0.42
                        0.68
                        3.22
                        0.93
                        1.36
                        1.78
                        4.38
                        2.25
                        19.92
                         0.15
                         0.00
 0.27
31.27
31.27
                                                              5.51
                                                              3.87
                                      15.60
                                                           0.887-1.113
                                                               0.000
                                                               0.906
                                                         13.44  0.915
                                                               0.931
                                                               0.937
                                                               0.940
                                                         10.30  0.958
                                                               0.982
                                                               0.991
                                                               0.994
                                                               1.002
                                                                1.005  OCDF
                                                      0.887-1.113
                                                          0.000
                                                      0.996-1.005
                                                          0.000
                                                   15.67  1.000 13C12-OCDD
                                                                                                       AN
IS3  Q
  Triangle Laboratories, Inc.® Analytical Services Division
  801 Caprtola Drive • Durham, North Carolina 27713
  Phone: (919) 544-5729 • Fax: (919) 544-5491
                                                                        Printed: 12:01 09/18/J
                                                                                      103

-------
Page No.
09/18/97
Listing of S975867B.dbf
Matched GC Peaks / Ratio / Ret.  Time
Compound/
M_Z....  QC.Log Omit Why  ..RT. OK Ratio Total.Area... Area.Peak.1..  Area.Peak.2.. Rel.RT Compound.Name..  ID.. Flags.
Column Description	  "Why" Code Description	  QC Log Desc.
M_Z   -Nominal Ion Mass(es)
. .RT. -Retention Time (mtn:ss)
Rat.l -Ratio of M/M+2 Ions
OK    -RO=Ratio Outside Limits
Rel.RT-Relative Retention Time
    End o f Report
       WL-Below Retention Time Window
       WH-Above Retention Time Window
       Sit-Below Signal to Noise Level
       
-------
 il»>S975867 tl-905 Aajtl3-SXP-1997 02tl2i56 XI+ Voltage SIS 70S HOimoift
 03.9016 T:3 BSOB(256,30,-3.0) PKD(9,5,S,O.OS\,272.0,1.00\,T,T)  KxptXPCUS
TRIANGLE LAIS  T*xt:0-N23-2 TLH43085                        XK7. TIMX -   02:15
                 19:00           20,00            21,00           22,00
 ile,S975867 tl-905 Acq,13-SXP-1997 02,12:56 XI+  Voltaye  SIX 70S Noif»,54
 05.8987 F:2 BSU»(256,30,-3.0) PKD(9,S,S,0.05\,216.0f1.00\,f,T)  XxpiXPCOS
TRIANGLE LABS  Tejct:O-M23-2 TLH430B5                        IKT.  TIMX -   02:15
 001
                 19:00            20:00           21:00            22,00
File,S975867  tl-905 Acq:13-SXP-1997 02,12,56 EH- Voltage SIX 70S Noiae:128
 15.9419 F,2  BSUB(256,30,-3,Q)  PKD(9,5,5,0.05\r512.0,1.00\,T, T) ElpsEPCUS
TRIANGLE LABS  Text:O-M23-2 TLI#43085                       ItU. TIME  -   02:15
  001

  sol

  50:

  40J
                                                      A2.33E4
                                                                        Al. 74X4
                                                                  A2.13E4
                                                           A1.28X4
                                                                                   23:00
                                                                                   23:00
                                                                                       A6. 73E5
                 19,00            20,00           31:00            22:00
 File:S9758S7 tl-905 Acq,13-SEP-1997 02,12:56 EI+ Voltage SIX  70S  NOiae,103
 317.9389 Fi2 BSUB(256,30, -3 . 0) PKD(9,5,5, 0. 05\,412. 0,1. 00\,r, T) ExpiEPCUS
 TSIANGLE LABS  Text:O-H23-2 TLHH3085                       JTWJ-.  TIKE -   02:15
 1003

  80:

  so:

  40:

  20:

   01           •  - - -           	i	(k__
                                                                                    23:00
                                                                                       A8.72E5
                 19:00            20:00            21:00            22:00            23:00
 rile:S975867 #1-905 Acq:13-SEP-1997 02,12,56 Eli-  Voltage SIX  70S
 330.9792 T:3 EzpiEPCVS
 TRIANGLE LABS  Text:0-M23-2 TLIt43085                       INJT.  TIKX -   02,15
 1001
.O.O.EO
    Time
                                                                                                     -2.4X5

                                                                                                     -.1. 9E5

                                                                                                     Ll.4E5

                                                                                                     1.9.4X4

                                                                                                     .4.7X4
                                                                                                      O.OEO
                                                                                                         Tia
                                                                                                     .3.2X5

                                                                                                     .2. 5E5

                                                                                                     .1. 9E5

                                                                                                     .1.3X5

                                                                                                     .6.3X4
                                                                                                       O.OEO
                                                                                                          Tim
                  19:00            20,00           21:00            22:00
 File,S975867 tl-905 Acq:13-SXP-1997 02:12:56 EH- Voltage SIX 70S
 375.8364 T:3 Xxp:XPCUS
 TXIANGLX LABS  Text:O-M23-3 TLIt43085                       XK7. TIME  -
 J004
                                                                                    23:00
                                                                            02:15
                  19:00
                                   20:00
                                                   21:00
                                                                    22:00
                                                                                     23,00
                                                                                                       105

-------
 ilo,S975867 tl-905 Acqtl3-SXP-1997  02:12:56 XI+ Voltage SIX 70S Noise:76
 19.8965 T:2 BSU3(256,30,-3.0) PKD(7, 5,3, 0.05\,304.0,1.00\,f,T) XxpiXTCUS
TRIANGLE LABS  Text:O-M23-2 TU#43085                       TJC7. TIMX "   02:15
                                                                        Al.0814
            20:00                21:00                22:00                23:00
 ile:S975867 tl-905 Acqtl3-SXP-1997 02:12:55 EI+ Voltage SIS 70S N6imei98
 21.8936 T:2 BSOB(256,30,-3.0)  PXD(7,5,3, 0.05\,392. 0,1. 00\,r,T) EzptSTCOS
TRIANGLE LABS  Text:O-M23-2 TLIt43085                       ISJ. TIMS -   02:15
 00>
        .0614
            20:00                21:00                22:00                 23:00
File:S975867  tl-905 Acqsl3-SEP-1997 02:12:56 EH- Voltage SIR 70S Noise:231
331.9368 F:2  BSUB(256,30, -3. 0)  PKD(7,5,3,0.051,924.0, 1.00\,F,T) Exp:£PCUS
TRIANGLE LABS TexttO-M23-2 TLH43085                       INJ. TIME  -    02:15
1003
  80:
  50:
  40:
  20:
 80:
 50:
 40:
 20:
  0.
                                                   A7.00X3
          A8.50E3
              \3.81C3
                  A4.55E3
                                                                 A3.63X3
                                                                               AM/
                                                                                                15.3*3
                                                                                                L4.0r3
                                                                                                .2.7X3
                                                                                                .1.3X3
                                                                                                lo.oxo
                                                                                                     Time
            20:00                21:00                22:00                23:00
rile:S975867 tl-905 Acq:13-SXP-1997 02:12:56 EI+ Voltage SIR 70S Noiae:64
333.9338 T:2 SSUB(256,30,-3.0) PKD(7, 5,3,0.05\,256.0,1.00\,f,T) Elp:EPCDS
TRIANGLE LABS  Text:O-M23-2 TLIt43085                       JWJ. TIME -   02:15
100]
 80:
 50:
 40:
 20:
  o:
            20:00                21:00                22:00                 23:00
rile:S975867 tl-905 Ac00
                                                                                                .2.4E5
                                                                                                -.1.9X5
                                                                                                .1.4X5
                                                                                                .9.6E4
                                                                                                14. 8X4
                                                                                                  O.OEO
                                                                                                     Tim-
                                                                                                  4.1E5
                                                                                                 .3.2X5
                                                                                                 12.4X5
                                                                                                 Ll. 5Z5
                                                                                                 .8.1X4
                                                                                                 LO.0X0
                                                                                                     Tim
                                                                                           23:42
                                                                                                 -1.6E6
                                                                                                 -1.3X6
                                                                                                 .9.4X5
                                                                                                 .6.3X5
                                                                                                 .3.1X5
                                                                                                  O.OEO
                                                                                                         106

-------
rile:S975B67 #1-905 Acqil3-3XP-1997 02tl2i56 EI+ VoltMym SIX 70S Nairn*>53
339.8597 Til BSVt(256, 30,-3.0)  PKD(7, 5,3, 0.05\,208.0,1.00\,r,T) ExpiETCOS
TMIAHSZJC LABS  Tttxt.O-M2.3-2  TLH43085                       XX7. TXMZ -   02*15
100*                                                                 A5\04X4
              34.00                 35.00
riles S975867  #1-905 Acq,13-SEP-1997 02:12tSS
                                                          25.00
                                                  Volt*9* SIX 70S Hoif*
341.8567 f,2 BSOB(256,30,-3.0) PKD(7, 5,3, 0.05\,208.0,1.00\,f,T)  ExpiEXCOS
TXIAWSZE LABS
1004
                T*xt:O-H23-2 TLIf43085
 80:
 50:
 40:
 20:
  o.
                                                              IKT.  TIKE
                                                                     A3.
                                                                                 27 tOO
                                                                        s52
                                                                            02/15
     A2.12E5
                                 A2.54E4  A1.76E4
                                                     A2.30E4
                                                                                  A6.39E5
              24.00                 25.00                 25.00        ,         37-00
rile,S975867 #1-905 Acq,13-SEP-1997 02,12,56 EH- Voltage SIX  70S Noiaas60
351.9000 T:2 BSOB(256,30,-3.0)  PKD(7,5,3,0.05\,240.0,1.00\,r,T) ExptEBCUS
TRIANGLE LABS  Text .-O-M3J-3 TLI #43085                       JNJ. TIKE-   02,15
100*                                                                A7.52E5

 80:

 50:

 40:

 20:
    : A6.03E4
              24:00                  25,00                  26,00                 27,00
rlle:S975867 #1-905 Acq,13-SEP-1997 02,12,56 EH- Voltage SIX 70S NOima,52
353.8970 r,2 BSUB(256, 30,-3 .0) PXD(7, 5, 3, 0. OS\,208. 0,1. 00\,T, T) ExptEPCOS
TSIANSLE LABS  Text,0-M23-2 TLH43085                        IXJ. TIME -    02.15
1004                                                               A6.79E5

  80:

  50:

  40:

  20.
     AB.92E4
                                                                                     .79E5
               24,00                 25,00                 26,00                  27,00
 rilesS975867 #1-905 Acq,13-SEP-1997 02,12,56 EH- Voltage SIX 70S
 330.9792  r,2 ExpsEPCOS
 TXIANGLE  LABS  Teit,O-M23-2 TLH430B5                        IXJ. TIME -   02,15
 1003)
                                                                   25.21
                                                                                                     _1.OE5

                                                                                                      •.8-.2E4

                                                                                                      .6.2X4

                                                                                                      '.4.1E4

                                                                                                      •-2.1E4

                                                                                                       O.OKO
                                                                                                      ,.2.9E5

                                                                                                      '.2.4ES

                                                                                                      -1. 8E5

                                                                                                      .1.2S5

                                                                                                      .5.9E4
                                                                                                        O.OEO
                                                                                                           Tim
                                                                                                       .2.7E5

                                                                                                       12.1Z5

                                                                                                       '.1.6ES

                                                                                                       ll.lES

                                                                                                       .5.4E4
                                                                                                        O.OEO
                                                                                                           Tim
   80:

   50:

   40.

   20:
                                                                           36,42
                                                                                                27,38
                                                           25,59
            23,53  34i10.
                                                                                                      ^3 . 8E6

                                                                                                      _J . OIT5

                                                                                                      -_2.3
-------
F3.J.e:S97Sa67 tl-905 Acqtl3-SXP-1997 Oitlit56 XI* Voltage SIX JOS Holme: 00
355.8546 Ti2 BSUB(256, 30, -3.0) PKD(7, 5,3, 0.05\,240. 0,1.00\,r,T) XxpiXPCUS
TKIAHGLX LASS Text,O-H23-2 TLI44308S 1X7. TZMX - 02,15
lOOt:
80.
60.
40.
20.
0.
A3. 34X5
h



/ - L *
24\48 25\bb 25*112 25T:24 25\36 '25\48 26\bo 26\12 26\24 26':36 26^48 27\'oO 27\'l2 27\24 27\36
.9.1X4
.7.3X4
.5.5X4
.3 . 7X4
.1 . 8X4
0.0X0
Time
rile ,3975867 #1-905 Acq,13-SXf-1997 02,12,56 EH- Voltage SIS 70S Koimei54
357.8516 F:2 BSUB(256, 30, -3.0) PKD( 7,5, 3, 0. 05\,216 . 0,1.00\,r,T) XxpiXPCUS
TRIANGLE LABS TmjctiO-M23-2 TLI#43085 IX J. TIME * 02:15
1004
80.
60.
40:
20:
o:
Al. 0X5

\

,
A It
I *\A8.90E3 1
AJ.4«tb A3.90E3 A/ V A A1.19X4
24:48 25:00 25:12 25:24 25:36 25:48 26:00 26:12 26:24 26:36 26:48 27:00 27:12 27:24 27:36
.3.3X4
.2.7X4
.2.0X4
.1.3X4
.6.6X3
0.0X0
Time
FileiS975867 #1-905 Acq:13-SEP-1997 02:12:56 Eli- Voltage SIS 70S N6iae,S6
367.8949 r,2 BSUB( 256, 30, -3 . 0) PKD(7, 5, 3, 0 . 05\,224. 0, 1 . 00\,f, T) ExpiEPCUS
TRIANGLE LABS Text:O-M23-2 TLI#43085 JKT. TIHX ' 02,15
ion.
so:
60:
40:
20:

0.
AS . 09X5




A9.11E4 I \

24,48 25,00 25,12 25:24 25,36 25:48 26:00 26,12 26:24 26,36 26,48 27:00 27:12 27:24 27,36
.2.3X5
'.1 . 8X5
.1 . 4X5
.9.2X4
'.4.6E4

' 0 . OEO
Time
rile:S975867 #1-905 Acq:13-SEP-1997 02:12:56 EI+ Voltage SIS 70S Unite, 58
369.8919 T:2 BSUB(256, 30, -3.0) PKD(7, 5,3,0 .05\,232. 0,1. 00\,r,T) Exp:EPCVS
TRIANGLE LABS TeJct:0-M23-2 TLH430SS INJ. TIME - 02,15
1003
80.
60.
40.

20.
0.
A3. 54X5
1



A2.06E5
A l\

24:48 25:00 25tl2 25:24 25:36 25:48 26:00 26:12 26,24 26:36 26:48 27:00 27:12 27:24 27:36
rl . 6E5
.1.3X5
.9.6X4
.6.4X4

.3.2X4

Tims
r±le>S975867 #1-905 Acq:13-SXP-1997 02:12:56 XI+ Voltage SIR 70S
330.9792 F:2 XxpiEPCUS
TRIANGLE LABS T*Xt,O-M23-2 TLI#43085 IKT. TIME - 02:15
lOOi


80.

60.
40.
20.
0.
\ 27i26
26:42 jf-c-, 27:05 A. /»./%. A.
26,21 26:36A 36>*3 "i" 27:16 \f^\ /\
25:59 /> /S^V\ J\ f\l\~f\J\ / * V
25:41 y/Vv/?f*l/ \f\ 1 \ 1 \f >/
25:00 ^^5,23 J\ f ^V^ V \ \l V

\s

r3.8X6


'.3.0X6

.2.3X6
.1.5X6
.7.6X5

24':48 25',00 25\12 25':24 2S\36 2S':48 26l,bb 26\12' 26\24' 26\ 36 ' jtfiifl' i?ioO ' 27\12 27',24 ' 27\ 36 Time

-------
 ila:3975867 H-346 Acq:13-SEP-1997  02,12,56 EI+ Voltage SIR 70S Noif*:498
 73.8308 T:3 BSUB(256r30,-3.0) PKD(7,5,3,0.05\,1992.0,1.00\,r,T) XxptXTCOS
TRIANGLE LABS  T*xttO-M23-3 TLH43085                        IHJ. TIMX  -  02:15
 OOJ

 80:

 50:

 40:

 20:                      A4.35X4
       28:12  28,24 28,36  28:48  29:00 29,13  29,24 29:36  29,48 30:00  30\12 30\24
 He-.8975867  #1-346 Acq:13-SEP-1997 02:12:56 EI+ Voltage SIR  70S Noift»491
 75.8178 F:3  BSUB(256,30,-3.0) PKD(7,5,3,0.05\,1964.0,1.00\,r,T) Xxp,EPCDS
TRIANGLE LABS  T*xt:O-H23-3 TLH43085                       IJKT. TIMX -   02,15
 00]

 80:

 50:

 40:

 20:
                         A3.11JE4
       28,12 28,24  28,36 28:48  29,00 29:12  29:24 29:36  29:48 30:00  30:12 30:24  30:36 30:48
rile:S975867 #1-346 Acq,13-SEP-1997 02,12:56 EI+ Voltage SIS  70S NOia*:316
 83.8639 F:3 BSUB(256,30, -3. 0)  PKS(7, 5,3, 0. 05\f1264. 0,1. 00\,r, T) Exp:EPCUS
TRIANGLE LABS  T*xt:O-M23-2 TLH43085                       IKJ. TIME -  02:15
1004
                 AS.48X3
                                          ,» A  _rfL_,
                                                AS. 83X3
                                                            Al .61X4
                                                                        . 05X3
                                                                                       A3.67Xf
                                                                                                     .8.4X4

                                                                                                     .6.7X4

                                                                                                     .5. t*4

                                                                                                     .3.3X4

                                                                                                     .1. 7X4
                                                                                                      .0.0X0
                                                                                            0i4« 31i««   ZlM
                                                                                                     .1.4X5

                                                                                                     Lt.AM

                                                                                                     ,7.0X4

                                                                                                     .3.3X4
                                                                                        A4.12S4
                                                                                   -Pi
                                                                                                      .a. oxo
 ao:
 so:
 4o:
 20:
  o:
                                                    A3.38E5
                          A4.91E4
                                                                   A2.67E5
                                                                                        A2.03X5
                                                                                                  31:00   Tim*
                                                                                             -2.0ES

                                                                                              l.fXS

                                                                                             ^1.2*5

                                                                                              .7.9X4

                                                                                              .4.0X4
       28:12  28:24 28:36  38:48 29:00 29:12  29:24  29:36  29:48 30:00  30:12 30:24
rile:S975867  tl-346 Acq:13-SEP-1997 02:12:56 EI+ Voltage  SIR 70S  »oiae:337
385.8610 Ts3  BSUB(256,30r-3.0) PKD(7,5,3,0.05\,134S.0,1.00\,r,T)  ExpsEPCVS
TRIANGLE LABS  Text:O-M23-2 TLI«43085                        INJ.  TIME -   02:15
                                                    A6.48E5
                                                                   A5.64E5
                                                                                     30:36 30:48
                                                                                                      .O.OEO
                                                                                                  31': 00   Tim*
 1003

  80:
  50:

  40:

  20:

   0.
                          A6.25S4
                                                                                        A3.68X5
                                                                                              -2.6S5

                                                                                              \.2.1E5

                                                                                              .1. 6E5

                                                                                              .1. OE5

                                                                                              .5.2E4
                                                                           -tH
        28,12 38,24  28:36 28,48  29,00  29:12 29,24  29:36 29:48  30:00 30:13  30:34
r±le:S975867 #1-346 Acq:13-SEP-1997 02,12:56 EI+  Voltage SIR 70S
392.9760 F:3 Xxp:EPCUS
TRIANGLE LABS  T*xt:O-M23-2 TLHH3085                        IJKT. TIME -   02:15
1003,
                                                                             30:20
                                            29:20
                                                                                     30:36  30:48
                                                                                                       .O.OEO
                                                                                                   31>00  Tim
  80:

  50:
  40:

  20:

   o:
                                                                                     30:34
                                                                                            30:47
      28:08
             28:21   28:36
                                                                                              .3.8E6

                                                                                              .3.0X6

                                                                                              '.3.3E6

                                                                                              1.1.5E6

                                                                                              .7.6X5
        38:13 38:34  28:36 28:48  29:00 29:13  39:34 39:36  39:48 30:00 30:13  30:34
 File:S975867 #1-346 Acgsl3-SEP-1997 03:12:56 EI+ Voltage SIR 70S
 445.7555 Ts3 Sxp:EPCUS
 TRIANGLE LABS  T*xt:O-M23-2 TLI#43085                       INJ. TIME '    02:15
 1001                      28 47

  80:

  60:

  40:

  30:

   0:
                                                                                     30:36  30:48
                                                                                                       O.OEO
                                                                                                   31': 00   Timm
                                                                                          30:44
                                                                                              .2.8X4

                                                                                              13.3X4

                                                                                              '•.1.7X4

                                                                                               a. 1x4

                                                                                               .5.6X3
                                                                                         JO.55
                                                                                               .0.0X0
28': 12  38:34 28:36  38:48 29s00 29\ 13  39',24 29',36  29',48 30',00  30:12 30:24  30:36 30:48  31:00   X*»

-------
 'i±e,S9758S7 11-346 Aoj:13-SXP-1997 02,12,56 XH- Voltage SIS 70S *oiie,-J7t>
 89.8156 r,3 BSUB(256,30,-3.0) PKD(7,5,3,0.05\,1104.0,1.00\,f,T) XrptXPCDS
TRIANGLE LABS  Te*t:O-M23-2  TLI443085                       OtJ. TIME  -   02,15
            AS.17X4
     28:36   28',48   29', 00    29', 12    29,24    29', 36   29', 48    30tOO   30', 12    30',24    30,36       Time
 iletS975867  tl-346 Aoqil3-SXP-1997 02,12,56 EH- Voltage 3IS  70S Hoi*e,331
 91.8127  r,3  BSOB(256,30,-3.0) PKD(7,5,3,0.05%,1324.0,1.00\,r,T) XxptXPCOS
TRIANGLE  LABS  Text:O-M23-2 TLH43085                       IKT. TIME -   0.3(15
  00$
           A3.85X4
    28': 36    28': 4 8   29': 00    29': 12   29': 24    29': 36   29': 4 8    30':00   30:12    30:24
rile-.S975867 tl-346 Acg:13-SEP-1997 02:12:56 EH- Voltage SIR 70S Soiaes387
 01.8558 r-.3 BSVB(2S6,30,-3.0)  PKD(7,5,3, 0. 05 \,1548. 0,1.00%,T, T) ExptEPCVS
TRIANGLE LABS   Teit:O-M23-2 TLH43085                       HtJ. TIME -    02:15
1001                                                                                 A5.
  80J

  so;

  40:

  20.
                                                                                          30:36
                                                                                          2E5
                                                                          A4.51E5
            Al.68X5
             A
                                                                                                      Time
 2.3X5

 1.9X5

LI. 4X5

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     28:36   28:48    29,00   29:12    29:24   29:36    29,48   30,00    30:12   30:24
rile:S975867 tl-346 Acq:13-SXP-1997 02,12,56 XI+  Voltage  SIR 70S Noiees443
403.8529  Ts3 BSUB(256,30,-3.0) PKD(7,5,3, 0.05*, 1772.0,1.00\,r,T) ExptEPCUS
TRIANGLE  LABS  Text:O-M23-2 TLIt43085                       INJ. TIME -   02:15
1001                                                                                A4.
    ;                                                                     A3.31E5
  ao:

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  40.

  20:
                                                                                          30:36
                                                                                          9X5
                                                                                                  .0.0X0
                                                                                                      Time
             A7.S4X4
                                                                       . /
                                                                                                   1. 7X5

                                                                                                   1.4X5

                                                                                                   1. 0X5

                                                                                                   6.9X4

                                                                                                  '.3.4X4
      28:36   28,48    29:00   29:12    29:24   29:36    29:48   30:00
 rileiS975867 tl-346 Acq:13-SEP-1997  02sl2:56 EI+  Voltage SIX 70S
 392.9760  n3 Kxp-.XPCUS
 TRIANGLE  LABS  Tsxt:O-M23-2 TLH43085                        INJ. TIME -   02:15

    *                                                                   30;
                                     29,20

                      28:        29'13
      28-.362B.1.44-      —
                                                                          30:12   30:24    30:36
                                                                                                   .0. OEO
                                                                                                      Time
      28:36    28:48
                       291 00
                                29> 12   29:24
                                                 29136
                                                         29,48
                                                                 30,00

-------
rlle,S975867 41-390 Acq:13-SEP-1997 02tl2tS6 EX+ Voltage SIS  70S Hoiie,811
407.7818 P:4 BSVt(256,30,-3.0) PKD(7,5,3, 0.051,3244.0,1.00\,f,T) XrptXPCOS
TRIANGLE LABS  Text,O-H23-2 TU443085                       IK7. TIME  -   02il5
1003k                              A4.59E4
                                                                                                       OMO
     31,48      32,00      32:12     32,24      32,36      32,48     33,00
rile:S975867 41-390 Acq,13-SEP-1997 02,12i56 EH-  Voltage Sit 70S Koiae,487
409.7789 fi4 BSUB(256, 30,-3.0 ) PKD(7, 5,3, 0.05\,1948.0,1.00\,F,T) SxpiSPCUS
TRIANGLE LABS   Text:0-M23-2 TU943085                       1WJ. TIME "   02,15
                                  A3.
                                                              OOE4
                                           33112
                                                     33124
      31:48      32': 00     32,12      32:24      32:36     32:48      33,00      33,12
 Tilt,:3975867 41-390 Acq:l3-SEP-1997 02,12,56 EH- Voltage SIX 70S Noise,639
 417.8253 f,4 BSUB( 256,30, -3. 0)  PKD( 7,5,3, 0. 05\,2S56. 0,1. 00\,r, T) SxpsEPCUS
 TRIANGLE LABS  Tejct,0-H23-2 TLI443085                       IJKT. TIME -   02:15
 100*              A1.35E5
                                                      33124
  80:

  60:

  40:

  20:
                                           A1.12E5
A8.53E4
             A1.29E4J
                            A9.19E3
                                              A1.38E4
                                                            A1.10E4
      31:48     32,00      32,12     32,24     32,36      32:48     33,00     33,12
 rileiS975867 41-390 Acq,13-SEP-1997 02:12:56 EH- Voltage SIR  70S B6iae:513
 419.8220 P:4 BSUB(256,30,-3.0) PKD(7,5,3,0.OS\,2052.0,1.00\,r,T) ExptEPCUS
 TRIANGLE LABS  Text,O-H23-2 TLI443085                       IK7. TIME -  02:15
 1001              A2.B9ES
                                                                                         33,24
  80:
  60:
  40:
  20:
                                                                              A2.66E5
                                   AS.95E4
                                   _/	v—
                          Al. 69E4
                                                    Al.64E4
                                                                    33,00
                                 32:19
     31:48     32,00      32,12     32,24      32,36      32,48
File,S975867 41-390 Acq,13-SEP-1997 02,12:56 EI+  Voltage SIR  70S
430.9729 F,4 ExpiEPCUS
TRIANGLE LABS  Text,O-M23-2 TLI443085                       JJTJ.  TIME -
100*                            ,,.,a       32,33        32,47
                      32:08
    ^A^v~v\y^
  fiOJ

  40:

  20:
   o.
                                                                               33,12
                                                                                         33,24
                                                                            02,15
                                                                                            33,27
       31,48      32,00     32,12      32:24     32:36     32:48      33,00     33:12      33,24
  rile:S975867 41-390 Ac
-------
 1J.0IS37SS67 U-J90 AcqIU-SfP-J.997  OillilSt EI+ Voltage SIX 70S
 23.7766 T:4 BSUf(256,30,-3.0)  PKD(7,5,3,0.05\,1172.0,1.00\,T,T) Exp:EPCDS
TXIANSLX LASS  Tejct:O-M23-2 TLH43085                       1X7. TIKE -
1001                         A6.04E4
   32:00  32t06   32:12  32ilB   32:24   32t30  32i36   32:42  32:48  32:54   33:00
rile:S975867  tl-390 Acq:13-SEP-1997 02:12:56 Eli- Voltage 3IX 70S Noite:309
425.7737 Tit  BSUB(256,30,-3.0)  PKD(7,5,3,0.05\,1236.0,1.00\,r,T) ExpiEPCUS
TRIANGLE LABS Text:0-M23-2 TLZt43085                       IKT. TIME  -    02:15
1003,                         A9.37E4
 80J

 so:

 40:

 20.
                   A1.55S4
          Al.65X4
                                                                                     A7.80S3
                                                    Al.06E4
                                        A3.54X3
                                                                                 37X3
.1.9X4

-1.5X4

.1.1X4

.7.7X3

.3.8X3
                                                                                                  0.0X0
                                                                                                    Timm
   32:00   32:06  32:12  32:18   32:24  32:30   32:36   32:42  32:48   32': 54   33:00
rile:S975867 tl-390 Acg:13-SEP-1997 02:12:56 EI+ Voltage SIX  70S Noiae:346
435.8169  F:4 BSUB(256, 30, -3 .0 ) PKD(7,5, 3, 0. 05\,1384. 0,1 . 00\, T, T) ExpsEPCUS
TRIANGLE  LABS  Text:O-M23-2 TLH43085                       JUT. TIME -   02:15
                                                                                    33:06  33:12
100$
  so:
  so:
  40:
  20:
                                                                  A2.31E5
                              A2.75E4
                                           A7.06E3
            T
                                                                                                r5.1E4

                                                                                                .7.3E4

                                                                                                IS. 5E4

                                                                                                -3.7E4

                                                                                                '.1. 8E4
                                                                          A1.58E4
                                                                                                /
   32:00  32:06   32:12  32:18  32:24   32:30  32:36   32:42   32:48  32:54   33:00
Tile:S975867 tl-390 Acqtl3-SEP-1997 02tl2i56 EI+ Voltage SIX 70S Noise, 14 5
437.8140 f:4 BSUB( 256 , 30, -3 .0 )  PKD( 7, 5, 3, 0 . 05%, 580. 0, 1 . 00\,F, T) Exp:EPCUS
TSIANSLE LABS  Text:O-M23-2  TLI#430BS                       IJTJ: TIME -   02:15
                                                                                     33:06  33:12
 .O.OEO
     Time
1003

 80.

 60.

 40.

 20.
   0_
                                                                  A2.QSE5
                 A7.07E3
                               A1.46E4
    32:00  32:06  32:12   32:18  32:24   32:30  32:36  32:42   32:48  32:54  33:00
 f±le:S97S867 tl-390 Acqs13-SEP-1997 02:12:56 EI+ Voltage SIX 70S
 430.9729 T:4 Exp:EPCDS
 TRIANGLE LABS  TextsO-M23-2  TLIf43085                       HKT. TIME -   02:15
                                                                                                 .O.OEO
                                                                                    33:06   33:12    Time
 .8.1E4

 -6.4E4

 -4.8E4

 -3.2E4

 _1. 6E4
 1004
                                            32;<33
    32:00  32:06   32:12  32:18  32:24   32:30  32:36   32:42  32:48  32:54
                                                                                       I i i i  i i I
                                                                                    33:06   33:12
  O.OEO
     Tim
                                                                                                        112

-------
ril»:S975867 #1-390 Aoqtl3-SXP-1997 02:12,56 XI+ VoltMgm SIX 70S Holtft 332
441.7428 Tt4 BSOB(256,30,-3.0) PKD(7, 5,3,0.05\,1328.0,1.00\,r,T) XxpiXPCDS
TRIANGLE LASS  T*xt,O-H23-2 TLH43085                       1X7. TXHX -   02tl5
10 0\
                         AS.51X4
                                                      A3.87X4
                                                                         AS.22X3
                                                                                   A2.30X4
                                                                  t^jful^
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J.3X4
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.1.4X4

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   8X3

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                   33,00
                                      33,00
                                                         34,00
                                                                            35,00
rile,S975867 tl-390 Acqil3-SXP-1997 02,12,56 EI+ Voltage SIS 70S Koimei512
443.7399 P,4 BSUB(256,30,-3.0)  PKD(7,S,3,0,05\,2048.0,1.00\,T,T) Exp:EPCUS
TRIANGLE LABS  TextsO-H23-2 TLIt43085                       HKT. TIMX '   02:15
100\                     A1.34E5
                    32i00              33:00              34:00
 rile:S975867 41-390 Acq:13-SEP-1997 02:12:56 EH- Voltage  SIR  70S
 430.9729 r,4 ExptEPCUS
 TRIANGLE LABS  Text:O-M23-2 TLH4308S                      INJ. TIME

                              32,33     33,03
                          32: IS
                                                                            35:00
                                                                                                     Time
                    32:00              33:00              34:00
 File:S975867 91-390 Acq:13-SEP-1997 02:12:56 XI+ Voltage SIR 70S
 513.6775 F:4 ExpiEPCUS
 TSIASSLX LABS  Text:0-H23-2 TLH4308S                      IWJ. TIME

-------
 'iJ.»:S97S867 #1-39O AoqiJ.J-SSP-J.997 OJHJ:56 El* VOJ\tMg» SIM 70S MOlM»:54
 57.7377 Ti4 BSUB(256,30,-3.0)  PXD<7,5,3,0.05\,216.0,1.00\,T,T) ElpifPCUS
TRIANGLE LABS  T+rttO-M23-2 TLH43085                       OUT. TOtf -   02il5
 00$
                                                    .55X4
             35il2         35,18         35:24         35t30         35:36
rile:S975867 #1-390 Aoqtl3-SEP-1997 02:12i56 EI+ Voltag» SIX  70S Nairn*t40
 S9.734B T:4 BSUB(256,30,-3.0) PKD(7,5,3,0.05\, 160.0,1.00\,T,T)  XxpttPCUS
TXIANGLK LABS   TmxttO-M23-2 TLH43085                       IJKT. TIMX -   02115
100\
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"^                   '   '                                         A5.00E3
              I  \      I   \        /\
401

20.
                                                                  35:42
                                                                               Al.78E3
              35i12         35:13         35i24         35:30         35:36
rile:S975867  #1-390 Acq:13-SEP-1997  02:12:56 EH-  Voltage SIR 70S Noiae:63
469.7779  T:4  BSU3(256,30,-3.0)  PKD(7,5,3, 0. OS\,252. 0,1. 00%,r,T) EzpsEPCtJS
TRIANGLE  LABS  Text:O-M23-2 TLI#43085                       JKT. TIME -   02:15
1001                               A1.56E5
  80.

  60.

  401

  20.
                                                                  35:42
              35:12         35:18         35:24         35:30         35:36
 File-.3975867 #1-390 Acqtl3-SEP-1997 02:12:56 EH- Voltage SIS 70S Jtoiae:70
 471.7750 T:4 BSU3(256,30,-3. 0)  PKD(7,5,3,0.051,280.0,1.00\,r,T) EiptEPCVS
 TRIANGLE LABS  Text:O-M23-2 TLI#43085                       INJ. TIKE -   02:15
 1004                              A1.57E5
  80J
  eo:
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                                                                  35:42
  20:
                                                            A1.10E4
              35:12         35:18         35:24         35:30         35:36
 r±le:S975867 #1-390 Acqil3-SEP-1997 02:12:56 EI+ Voltage SIR  70S
 430.9729 r:4 ExptSPCUS
 TRIANGLE LABS  Taxt:O-M23-2 TLI#43085                       ISJ.  TIME -
                                                                   35:42
 1003

  80.

  60.

  40.

  20.

   0.
                                                                             02:15
35:13
                     35:22
                                                       35:37
                                                                      35:44
              35tl2
                             35:18
                                          35:24
                                       351:30
                                                                      35:36
                                                                                  "•—I  '
                                                                                   35:42
                                                                                 5.1E3

                                                                                 4.1E3

                                                                                 3.1X3

                                                                                 .2.1E3

                                                                                 .1. OE3

                                                                                 .O.OEO
                                                                                    Time
                                                                                -5.6E4

                                                                                -4.5E4

                                                                                -3. 4E4

                                                                                 .2.3E4

                                                                                 -1.1E4
                                                                                 .O.OEO
                                                                                     Tim
                                                                                                _3.6E6

                                                                                                -2.8E6

                                                                                                -2.1S6

                                                                                                .1.4X6

                                                                                                '.7.1X5
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   Tim
                                                                                                          114

-------
Channel    I  338,9792    Peak top
Height   2,32 volts  Span   288 ppi

Systei file naie            EPCUS2
Data   file naie         R'9913971
Resolution                  18888
Groupnmber                     2
lonlzatlon iode               Eh
Switching                 VOLTflGE
Ref, lasses   292,9825,   416,9768
             J   331     S   368
             K   332     1   378
             L   334     U   376
             H   348      V   418
             H   342
             0   352
             P   354
             0  356
             R  358

      &as!    416,9768     Peak top
  heloht    ,£ volts Spar   286 ppi
                                                                    115

-------
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53.8970 F:2 Exp.-EPCUS
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-------
•'His 15975867 #1-346 Acq:13-SEP-19g7 02:12:56 EI+ Voltage SIR 70S
173.8208 P:3 Exp:EPCUS
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LOO*                  28 49

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                           29:00                         30:00
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183.8639  F:3  Exp:EPCUS
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L00%                                           29:37
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-------
.le:S975867  #1-390 Acq: 13-SEP-1997 02:12:56 EI+ Voltage  SIR 70S                 ~~~~~
.7.8253  F:4  Exp:EPCUS
unple Text:0-M23-2 TLI#43085                        INJ.  TIME =    02:15  File  Text:O-M23
                   32:05
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.9.8220  F:4 Exp:EPCUS
unple  Text:0-M23-2 TLI#43085                        INJ.  TIME =    02:15  File  Text:O-M23
                   32; 05
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                                                                                           Time

-------
 Lle:S975867  #1-346 Acq:13-SEP-1997 02:12:56 EI+ Voltage SIR 70S
 73.8208  F:3  Exp:EPCUS
 ample Text:O-M23-2 TLI#43085                       INJ.  TIME =
                      28  49
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                                                                                        1.7E4
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75.8178 F:3 Exp:EPCUS
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                                                                                          Time
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45.7555 F:3 Exp:EPCUS
ample Text:O-M23-2 TLI#43085                       INJ. TIME =   02:15 File Text:O-M23
00%                 28;47                                                    30:44
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                                                                                           Time

-------
 le:S975867 #1-346 Acq:13-SEP-1997  02:12:56 EI+ Voltage  SIR 70S
 3.8208 F:3 ExprEPCUS
 .mple Text:0-M23-2 TLI#43085
    INJ. TIME =
                           02
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'5.8178  F:3 Exp:EPCUS
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Lle:S975867 #1-346 Acq:13-SEP-1997 02:12:56 EI+ Voltage SIR 70S
15.7555  F:3 Exp:EPCUS
unple  Text:0-M23-2 TLI#43085                       INJ. TIME =   02
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-------
 Lle:S975867  #1-346 Acq:13-SEP-1997  02:12:56 EI+ Voltage SIR 70S
 '3.8208 F:3  Exp:EPCUS
 unple Text:O-M23-2 TLI#43085
 30%
sol
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                    30:36        30:42
                   INJ.  TIME =   02:15  File  Text:0-M23-2 TLI#4
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       30:24         30:30
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'5.8178 F:3  Exp:EPCUS
imple  Text:O-M23-2 TLI#43085                       INJ. TIME =   02:15 File Text:O-M23-2 TLI#4»
                                                   30:44
                        I	1	?	1	1	1	1	1	1	1	1	
       30:24'       30:30        30:36        30:42        30:48        30:54              Time
.le:S975867  #1-346 Acq:13-SEP-1997 02:12:56 EI+ Voltage SIR 70S
15.7555 F:3  Exp:EPCUS
imple Text:O-M23-2 TLI#43085                       INJ. TIME =   02:15 File Text:O-M23-2 TLI#4»
)0%                                                 30;44
      30:24
      30:30
30:36
30:42
                                                           30:48
30:54
Time

-------
TLI Project:     43085
Client Sample:   O-M23-3
Method 23 PCDD/PCDF Analysis (a)
            Analysis File:   S975868
Client Project:
Sample Matrix:
TLI ID:

Sample Size:
Dry Weight:
GC Column:
S413-004
M23Train
181-55-3ABE

1.000
n/a
DB-5

Date Received:
Date Extracted:
Date Analyzed:
Dilution Factor:
Blank File:
Analyst:

09/03/97
09/04/97
09/13/97
n/a
S975815
ML

Spike File:
ICal:
ConCal:
% Moisture:
% Lipid:
% Solids:

SPX23704
SF56117
S975861
n/a
n/a
n/a
Analytes • •:•".".'.• ••^•'•••- '"•

2,3,7,8-TCDD
1,2,3,7,8-PeCDD
1,2,3,4,7,8-HxCDD
1,2,3,6,7,8-HxCDD
1,2,3,7,8,9-HxCDD
1,2,3,4,6,7,8-HpCDD
1,2,3,4,6,7,8,9-OCDD
2,3,7,8-TCDF
1,2,3,7,8-PeCDF
2,3,4,7,8-PeCDF
1,2,3,4,7,8-HxCDF
1,2,3,6,7,8-HxCDF
2,3,4,6,7,8-HxCDF
1,2,3,7,8,9-HxCDF
1,2,3,4,6,7,8-HpCDF
1,2,3,4,7,8,9-HpCDF
1,2,3,4,6,7,8.9-OCDF
Totals '•• ."/' :Jr ..V'.
Total TCDD
Total PeCDD
Total HxCDD
Total HpCDD
Total TCDF
Total PeCDF
Total HxCDF
Total HpCDF
•;-;--;::7:.'Amt.-ing)
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
: :; : Amt (n§)
ND
ND
ND
ND
ND
EMPC
ND
ND
Dt EMPC fta*k» at Flag*
0.01 	
0.01 	
0.02 	
0.02
0.02 	
0.03 	
0.10 	
0.006
0.01 	
0.01 	
0.01 	
0.01 	
0.01 	
0.01 	
0.02 	
0.03 	
0.07 	
: Number Dt EMPC Ftegs
0.01 	
0.01 	
0.02 	
0.03 	
0.006
0.02 	
0.01
0.02
                                       Page 1 of 2
                                                                        X237 J-SR »100. LARS tlO.04
Triangle Laboratories, Inc.®
801 Caprtola Drive • Durham, North Carolina 27713
Phone: (919) 544-5729 • Fax: (919) 544-5491
                       Printed: 13:19 09/18/97
                               122

-------
TLI Project:      43085
Client Sample:   O-M23-3
Method 23 PCDD/PCDF Analysis (a)
             Analysis File:  S975868
i Internal Standards
13C,:-2,3,7,8-TCDF
13C,2-2,3,7,8-TCDD
13C,2-l,2,3,7,8-PeCDF
13C,2-l,2,3,7,8-PeCDD
1JC,2-l,2,3,6,7,8-HxCDF
3CP-l,2,3,6,7,8-HxCDD
13C,2-l,2,3,4,6,7,8-HpCDF
13C,2-l,2,3,4,6,7,8-HpCDD
13Cir 1,2,3 A6,7,8,9-OCDD
Surrogate Standards (Type A)
37CL,-2,3,7,8-TCDD
13C,2-2,3,4,7,8-PeCDF
13Cp-l,2,3,4,7,8-HxCDF
13d2-l,2,3,4,7,8-HxCDD
13C,2-l,2,3,4,7,8,9-HpCDF
Alternate Standards (Type A)
13C,2-l,2,3,7,8,9-HxCDF
13C,2-2,3,4,6,7,8-HxCDF

Amt. (ng)
4.5
3.8
3.7
4.0
4.1
3.7
2.6
2.6
2.5
AmL (ng)
4.0
3.7
3.4
3.3
3.5
Amt (ng)
3.4
3.8
% Recovery
114
95.4
91.9
100
103
92.2
64.7
63.8
31.6
:-\.--:-~&£*Mmw
101
93.4
85.0
83.2
86.7
•<& Recovery
....•-:•. •:.^*.-??-rVove'y
84.8
94.6
QC Limits
40%- 130%
40%- 130%
40%- 130%
40%-130%
40%- 130%
40%- 130%
25%- 130%
25%- 130%
25%- 1 30%
QC Limits
70%-140%
70%- 140%
70%- 140%
70%- 140%
70%- 140%
: QC Limits
40%- 130%
40%- 130%
Ratio
0.74
0.77
1.36
1.50
0.50
1.22
0.43
1.04
0.91
'-. Ralte: ^j.
1.49
0.50
1.27
0.44
'•••• -Ratio- ,'.;;.••
0.52
0.51
«T^
21:37
22:22
25:41
26:44
29:17
29:58
31:56
32:46
35:20
'*•*&:?•*
22:23
26:23
29:11
29:54
33:08
; RT
30:29
29:46
*''**>
	
,;^flags,.
i
Flags
—
Recovery Standards ;?t ; "•••• -• •"•-.!•. -• ="- :• " -::': :^^^JV./-:.:?: ••'••••;v •••/. v ;•; ;.-.' . . ..-.' • -.•' RatfoV-^ifl.V-ilf. •• ;v;rkv;Fiags.
13Ci2-l,2,3,4-TCDD
13C12-l,2,3,7,8,9-HxCDD



0.83
1.22
22:10
30:16
—
                     Data Reviewer
                                        Page 2 of 2
             09/18/97
                           X237.PSR vlOO. LAW 6.K
 Triangle Laboratories, Inc.®
 801 Caprtola Drive • Durham, North Carolina 27713
 Phone: (919) 544-5729 • Fax: (919) 544-5491
                       Printed: 13:19 09/tW
                               123

-------
                       Initial
                                  ... Date...
Data Review By:
 ~&-     °\  I I%/)T Calculated Hois* Area:    0.93
The Total  Area  for each peak with an ion abundance ratio outside
ratio limits has been recalculated according to method requirements.
Page No.
09/18/97
Listing of S975868B.dbf
Matched GC Peaks /  Ratio  / Ret. Time
Compound/
M_Z....  QC.Log omit  Why
.RT. OK .Ratio Total.Area... Area.Peak.1.. Area.Peak.2..  Re1.RT Compound.Name.. ID.. Flags.
TCDF
304-306
 304-306

DC
DC
DC
DC
DC
DC
DC
DC


NL
SN
SN
SN
SN
SN
SN
SN
0

0:00
18:24
19:30
20:14
20:35
20:51
21:12
21:37
Peaks
0.

RO

RO
RO

RO
RO

65-
0.
1.
0.
0.
0.
0.
0
0

•0.89
85
24
,71
.41
.50
.74
.90
.63


0.
0.
2.
2,
2
1
3
5
0

24
.89
.04
.05
.46
.97
.27
.03
.00
                                                    0.838-1.092
                                                        0.000
                                                        0.851
                                                        0.902
                                                        0.936
                                                        0.952
                                                        0.965
                                                        0.981
                                                                                 1.000 2378-TCDF
                                                                                                      AN
 13C12-TCDF                     0.65-0.89
 316-318         DC  NL   0:00 RO  0.93           0.27
                        21:10 RO  1.06           5.52
                        21:37     0.74       1,205.98
 316-318               2 Peaks               1,211.50
                                     3.30
                                   514.33
    0.954-1.046
        0.000
  3.12  0.979
691.65  1.000  13C12-2378-TCDF ISO
 TCDD
 320-322
 320-322

DC
DC
DC
DC
DC
DC
DC
DC
DC
DC
DC
DC
DC
DC
DC
DC


NL
SN
SN
SN
SN
SN
SN
SN
SN
SN
SN
SN
SN
SN
SN
WH
0

0:
19:
20:
20:
20:
21:
21:
21:
22:
22:
22
22
22
23
23
23
Pe,

00
57
04
16
52
01
14
;36
:05
:23
:37
:46
:52
:07
:27
:47
aks
o.<

RO
RO
RO
RO
RO
RO
RO
RO
RO


RO
RO
RO
RO

55-
0.
0.
2.
0.
1.
1.
1.
1,
3,
0
0
0
0
2
2
0

0.89
79
44
93
17
55
09
.47
,45
.75
.52
.68
.68
.59
.82
.08
.50

                                       Above:  TCDF  / TCDD Follows
                       0.25
                       0.57
                       0.50
                       0.16
                       0.35
                       1.03
                       0.60
                       0.71
                       0.57
                       1.70
                       0.52
                       0.69
                       0.62
                       0.39
                       1.29
                       0.97
                       0.00
     .875-1.055
        0.000
        0.392
        0.897
        0.906
        0.933
        0.940
        0.949
        0.966
        0.987
        1.001 2378-TCDD
        1.011
        1.018
        1.022
        1.034
        1.048
        1.063
 37C1-TCDD
 328
                 DC  NL   0:00
                 DC  WL  19:47
                 DC  WL  19:57
                 DC  SN  20:41
                 DC  SN  20:58
                        0.38
                        0.74
                        0.32
                        1.56
                        0.97
      .910-1.090
         0.000
         0.885
         0.892
         0.925
         0.937
Triangle Laboratories, Inc.®  Analytical Services Division
801 Capitola Drive • Durham, North Carolina 27713
Phone: (919) 544-5729 • Fax: (919) 544-5491
                                                                       Printed: 13:20 09/18/97
                                                                                   124

-------
 Page Ho.     2

 09/18/97


 Compound/

 M_Z	 QC.Log Omit Why
Listing of S975868B.db£
Matched GC Peaks  / Ratio
                        / Ret. Tine
..HP. OK Ratio Total.Area...  Area.P.aJc.l..  Ar.a.Peak.2..  R.1.RT Compound.Name..  ID.. Flag,.
328
13C12-TCDD
332-334





332-334
PeCDF
340-342











340-342
13C12-P6CDF
352-354







DC
DC
DC
DC
DC
DC
DC
DC
DC
DC
DC
DC

DC
DC
DC

DC
DC
DC
DC
DC
DC
DC
DC
DC
DC
DC
DC
DC
DC
DC
DC
DC
DC
DC
DC
SN
SN
SN
SN
SN
SN
SN
SN
1
NL
WL
WL
SN

SN
SN
3
NL

SN
SN
SN
SN
SN
SN
SN
SN
SN
SN
SN
SN
1
NL
SN
SN
SN
SN
SN
SN
SN
21:38
21:42
21:59
22:09
22:23
22:53
23:14
23:29
23:42
Peak
0:
19:
20:
22:
22:
22:
22:
22:
00
;52
17
10
:22
32
42
56
23:00
Peaks
0:
23:
23:
24:
24:
25:
25:
25;
26:
26;
26:
27:
27:
:00
41
:56
49
:59
14
:23
:59
:17
:27
:43
:01
:17
27:34
Peak
0;
23
24
24
25
25
25
25
26
:00
:40
:13
:18
:09
:21
:57
:05
0.
RO
RO
RO
RO
RO
RO
RO
1.
RO
RO
RO
RO
RO
RO

RO
RO
RO
RO
RO
RO
1.
RO
RO
RO
RO

RO
RO

65
2
2
2
0
0
1
1
1
0
32
1
0
0
2
2
0
1
0
0
1
0
0
0
8
32
0
0
3
0
1
3
1
1
1
-0.89
.90
.25
.20
.83
.77
.81
.13
.07
.55
1,
-1.78
.14
.66
.65
.05
.00
.81
.74
.95
.30
.74
.42
.44
.95
.25
-1.78
.92
.44
.94
.79
.76
.34
.36
.01
.51
0
1
0
1
695
1
0
0
0
695
0
1
0
805
818
1
13
0
1
,636
Ten
i "w U
0
4
0
2
0
0
0
1
1
2
0
0
1
0
4
0
0
0
0
1
3
838
4
1
.79
.22
.84
.28
•96 695.96
.03
.72
.92
.76
.96
.51
.13
.80
•02 364.99
•51 356.56
.22
•42 3.54
.53
.01
.95
.26
•59 2.79
.71
.09
.54
.43
.96
.66
.02
.22
.41
.74
.37
.41
.59
.20
.56
.41
.25
.35
.11
•49 482.87
.06
.18
0.
0.
0.
0.
1.
1.
1.
1.
1.
,967
970
983
990
001 37C1-TCDD SUR1
023
039
050
060
0.910-1.090
0.000
0.
0.
440.03 0.
461.95 1.
1.
7.58 1.
1.
1.
0.915-
0.
4.24 0.
0.
0.
0.
0.
0.
1.
1.
1.
1.
1.
1.
1.
0.844-
0.
0.
0.
0.
0.
0.
355.62 1.
1.
1.
388
907
991 13C12-1234-TCDD RSI
000 13C12-2378-TCDD IS1
007
015
025
028
1.074
000
922
932
966
973
982
988
012
023
030 23478-PeCDF AN
040
052
062
073
1.156
000
921
943
946
979
987
000 13C12-PeCDF 123 IS2
010
016
Triangle Laboratories, Inc.®  Analytical Services Division
801 Capitola Drive • Durham, North Carolina 27713
Phone: (919) 544-5729 • Fax: (919) 544-5491
                                                                  Printed: 13:20

-------
Page  No.     3
09/18/97


Compound/
M_Z.... QC.Log Omit  Why
Listing of S975868B.dbf
Matched GC Peaks / Ratio  / Ret. Time
.RT. OK Ratio Total.Area... Area.Peak.1.. Area.Peak.2..  Rel.RT Compound.Name..  ID..  Flags.
N
352-354
PeCDD
356-358








356-358
13C12 -PeCDD
368-370







368-370
HxCDF
374-376












374-376
13C12-HXCDF
384-386


DC
DC
26:23
SN 27:12
SN 27:32 RO
2 Peaks
1.49
1.45
0.67
1
* W A..A _
1.32-
DC
DC
DC
DC
DC
DC
DC
DC
DC


DC
DC
DC
DC
DC


DC


DC
DC
DC
DC
DC
DC
DC
DC
DC
DC
DC
DC
DC


DC
DC
DC
NL
WL
SN
SN
SN
SN
SN
SN
WH
0

NL
SN
SN
SN
SN


SN
2

NL
SN
SN
SN
SN
SN
SN
SN
SN
SN
SN
WH
WH
0

NL
SN
SN
0:
24:
25:
25:
26:
26:
26:
27:
27:
00
44
04
22
09
18
28
13
27
RO
RO
RO
RO
RO
RO
RO
RO
RO
1.
4.
4.
9.
0.
6.
3.
3.
0.
- jujwvw ;
1.78
18
27
33
89
70
89
08
80
15
Peaks

0:
24:
25:
26:
26:
26:
26:
27:

00
42
20
02
17
44
54
27
1.
RO
RO
RO

RO


RO
759.27 454.30
1.15
0.92
,597.76

0.
0.
0.
0.
0.
0.
0.
0.
0.
0.

21
28
54
23
82
92
66
38
15
00
32-1.78
1.
3.
0.
1.
0.
1.
1.
00
11
67
75
18
50
.48
0.51
Peaks

0
28
28
28
28
29
29
29
29
30
30
30
30

:00
:13
:22
:40
:49
:11
-.16
:23
:36
:22
:30
:48
:55
1.

RO
RO
RO
RO

RO

RO
RO
RO
RO
RO

0.
0.
0.
0.
20
48
51
55
0.44
513.
40.
20 307.56
.92 24.43
0.81
554
W-./TM
05-1.43
1
1
1
0
1
1
1
1
1
0
0
1
0
.40
.57
.02
.84
.60
.25
.86
.37
.51
.99
.76
.78
.94
Peaks

0
28
28

:00
:21
:35
0
RO
RO

1
1
3
0
1
2
2
1
1
1
1
1
1
0
.12

.56
.41
.00
.69
.46
.36
.02
.23
.41
.39
.61
.01
.10
.00
.43-0.59
0
0
0
.65
.42
.54
1
1
1
.37
.07
.20
304.97 1.027 13C12-PeCDF 234 SUR2
1.059
1.072
0.926-1.024
0.
0.
0.
0.
0.
0.
0.
1.
1.

000
925
938
949
978
984
990
018
027

0.850-1.150
0.
0.
0.
0.
0.
205.64 1.
000
924
948
974
983
000 13C12-PeCDD 123 IS3
16.49 1.006
1.027


0.959-1.050
0
0
0
0
0
0
0
1
1
1
1
1
1

0.863
0
0
0
.000
.964
.969
.979
.984
.997 123478-HxCDF AN
.999
.003
.011
.037
.042 123789-HXCDF AN
.052
.056

-1.137
.000
.968
.976
Triangle Laboratories, Inc.® Analytical Services Division
801 Caprtola Drive • Durham, North Carolina 27713
Phone: (919) 544-5729 • Fax: (919) 544-5491
                                                                    Printed: 13:
97

-------
 Page No.
 09/18/97
Listing of S975868B.dbf
Matched GC Peaks / Ratio /
                                                Rat. Time
 Compound/

 M_Z.... QC.Log Omit Why ..RT. OK Ratio Total.Area... Ar.a.Peak.1.. Area.Peak.2..  Rel.RT Compound.Name. . ID.. Flag,.









384-386
HXCDD
390-392










390-392
13C12-HXCDD
402-404










402-404
HpCDF
408-410





408-410
DC


DC

DC
DC

DC


DC
DC
DC
DC
DC
DC
DC
DC
DC
DC
DC


DC
DC
DC
DC
DC


DC

DC
DC


DC
DC
DC
DC
DC
DC
DC

SN


SN

SN
SN

SN
4

NL
SN
SN
SN
SN
SN
SN
SN
SN
WH
WH
0

NL
WL
WL
SN
SN


SN

SN
SN
3

NL
WL
SN
SN
SN
SN
SN
0
29:01
29:11
29:17
29:34
29:46
30:03
30:16
30:29
30:37
Peaks

0:00
29:18
29:24
29:33
29:53
29:59
30:07
30:15
30:22
30:38
30:41
Peaks

0:00
28:36
28:41
29:00
29:23
29:54
29:58
30:06
30:16
30:27
30:41
Peaks

0:00
31:45
31:52
32:11
32:24
33:08
33:15
Peaks
RO


RO

RO
RO

RO

1.
RO
RO
RO
RO
RO
RO

RO
RO
RO
RO

1.
RO
RO
RO
RO



RO

RO
RO

0,
RO
RO
RO
RO
RO
RO

0.
0.
0.
0.
0.
0.
0.
0.
0.

91
50
50
19
51
16
23
52
81

05-1.43
0.
3.
1.
0.
2.
2.
1.
0.
0.
0.
0.

05-
1.
0.
2.
1.
1.
1.
1.
0.
1.
0.
0.

54
87
03
71
23
41
42
27
47
35
44

1.43
51
60
17
73
30
27
22
95
22
62
91

0.
529.
649.
0.
551.
0.
0.
429.
1.
51
99 176.72
92 217.16
41
11 184.95
36
86
21 146.08
34
0.
353.27 0.
432.76 1.
1.
366.16 1.
1.
1.
283.13 1.
1.
2,160.23

0.
0.
0.
0.
0.
0.
1.
0.
0.
0.
1.
0.

1.
0.
0.
1.
2.
388.
479.
1.
522.
0.
1.
1,390.
.88-1.20
1.
2.
7.
0.
2.
0.
3.

83
50
12
61
23
88
02

1.
0.
2.
2.
1.
2.
2.
0.
85
34
60
81
29
65
60
25
98
67
46
00

32
87
94
01
51
14 216.84
40 263.42
41
49 286.75
70
63
03

94
73
18
30
06
.07
,06
00
0.953-
0.
0.
0.
0.
0.
1.
1.
1.
1.
1.
1.

0.967-
0.
0.
0.
0.
0.
171.30 0.
215.98 1.
1.
235.74 1.
1.
1 .

0.995-
0.
0.
0.
1.
1.
1.
1 .

991
997 13C12-HXCDF 478
000 13C12-HXCDF 678
010
017 13C12-HXCDF 234
026
034
041 13C12-HXCDF 789
046

1.014
000
978
981
986
997 123478-HxCDD
001 123678-HxCDD
005
009 123789-HxCDD
013
022
024

1 . 033
000
954
957
968
981
998 13C12-HXCDD 478
000 13C12-HXCDD 678
004
010 13C12-HXCDD 789
016
024

1.042
000
994
998
008
015
038 1234789-HpCDF
041


SOR3
IS4

ALT2


ALT1







AN
AN

AN










SUR4
IS5

RS2









AN

Triangle Laboratories, Inc.® Analytical Services Division
801 Caprtola Drive • Durham, North Carolina 27713
Phone: (919) 544-5729 • Fax: (919) 544-5491
                                                                 Printed: 1320 09/18/$
                                                                               127

-------
Page No. 5
09/18/97
Compound/
M_Z .... QC . Log
13C12-HpCDF
418-420
418-420
HpCDD
424-426



424-426
13C12-HpCDD
436-438



436-438

OCDF
442-444










442-444
OCDD
458-460


458-460
13C12-OCDD
470-472

Omit
DC
DC

Listing of S
Matched GC I
Why . .RT. OK Rati
0.37-(
NL 0: 00 RO O.I
31:56 0.'
SK 32:47 0.:
33:08 0.'
2 Peaks




0.88-
DC
DC
DC
DC


DC

DC
DC




DC
DC
DC
DC
DC
DC
DC
DC
DC
DC
DC


DC
DC
DC


DC
DC
NL
WL
SN
SN
0

NL

SN
SN
1



NL
WL
SN
SN
SN
SN
SN
SN
SN
SN
SN
0

NL
SN
SN
0

NL
WL
0:00
31:58
32:09
32:46
Peaks

0:00
32:46
33:03
33: 16
Peak



0:00
31:17
31:55
32:32
33:00
33:23
33:58
34:38
34:51
35:13
35:28
Peaks

0:00
35:19
35:46
Peaks

RO
RO
RO
RO

0.
RO

RO
RO



0.
RO
RO

RO
RO
RO
RO
RO
RO
RO


0
RO

RO

0
0:00 RO
35:04 RO
35:20
470-472
1.
2.
2.
0.

88-
2.
1.
2.
0.



I975868B.
>eaks / R
Lo Total.
).51
53
13
37
14
- Above :
1.20
86
09
53
26

1.20
11
04
44
80

• - Above :
dbf
atio /
Area. .
2.:
299. f
1.1
200.:
500.:
HpCDF

1 Ret. Time
. Area. Peak. 1. . Area . Peak . 2 . . Re l.RT Compound. Name. . ID..
0.937-1.125
28 0.000
S9 90.77 209.12 1.000 13C12-HpCDF 678 IS6
SO 1.027
37 61.08 139.29 1.038 13C12-HpCDF 789 SUR5
26


0.88
1.
0.
1.
0.

0.
271.
1.
1.
271.
31
61
08
00

94
50 138.72
65
33
50
HpCDD / Octa-CDD and CDF
76-1.02
1.
3.
0.
2
0
3
0
0
2
0
0

.76
2
0
9

,07
.65
.81
.26
.66
.00
.68
.47
.75
.40
.78

-1.02
.59
. 83
.43

1.
0,
1.
0
2.
0
1
2
1
0
3
0

0
4
0
0
34
.81
.86
.95
.29
.68
.55
.31
.59
.96
.52
.00

.42
.47
.13
.00
.76-1.02
3
.44
2.49
0.91
1 Peak
0
2
171
171
.17
.00
.61 81.81
.61

0.977-
0.
0.
0.
1.

0.969-
0.
132.78 1.
1.
1.




1.005
000
976
981
000 1234678-HpCDD AN

1. 031
000
000 13C12-HpCDD 678 IS7
009
015



0.887-1.113
0.000
0.885
0.
0
0
0
0
0
0
0
1

0.887
0
1
1

.903
.921
.934
.945
.961
.980
.986
.997
. 004 OCDF AN

-1.113
.000
.000
.012

0.996-1.005
0
.000
0.992
89.80 1

.000 13C12-OCDD IS8

                                                                                            Flags.
Triangle Laboratories, Inc.® Analytical Services Division
801 Capitola Drive • Durham, North Carolina 27713
Phone: (919) 544-5729 • Fax: (919) 544-5491
Printed: 13:20 09/18/97
             128

-------
Page No.
09/18/97
Listing of S975868B.dbf
Matched GC Peaks  /  Ratio / Ret. Time
Compound/
M_Z....  QC.Log Omit Why  ..RT. OK Ratio Total.Area... Area.Peak.1.. Area.Peak.2..  Rel.RT Compound.Name.. ID.. Flags.
Column Description	  "Why" Code Description	  QC Log Desc.
M_Z   -Nominal Ion Mass(es)
..RT. -Retention Time (mm:ss)
Rat.l -Ratio of M/M+2 Ions
OK    -RO=Ratio Outside Limits
Rel.RT-Relative Retention Time
 *** End of Report
       WL-Below Retention Time Window
       WH-Above Retention Time Window
       SN-Below Signal to Noise Level
       
-------
 ile:S975868 #1-905 Acqtl3-SXP-1997 02i52i21 XI* Voltage SIX 70S Hoift 157
 03.9016 Ti2 BSUB(256,30,-3.0)  PKD(9,5,5,0.05\,228.0,1.00\,r,T) XxptXTCUS
TRIANGLE LABS  TeJCt:O-M23-3 TZH43085                       IJKT. TIMX -    0.2«55
 001
                 19.00            20-00           21.00            22:00
 lie:5975858 #1-905 Acq:13-SEP-1997 02:52:21 XI+ Voltage SIX 70S Noi*e:67
 05.8987 f:2 BSUB(256, 30,-3.0) PKD(9,5,5, 0. 05\,268. 0,1.00\,T,T) ExpiEPCUS
TRIANGLE LABS  Text:O-M23-3 TLH43085                       IKT. TIME  -    02:55
                                                                                    23100
                                                                                                      .0.0X0
                                                                                                          Time
                 19:00            20:00            21:00           22:00            23:00
File:S9758S8  #1-905 Acq:13-SEP-1997 02:52:21 XI*  Voltage SIR 70S Noise:69
  15.9419  r-.2  BSVS(256,30,-3.0) PKD(9,5,5, 0. 05\,276. 0,1. 00\,T, T)  Exp:SPCUS
TRIANGLE  LABS  Text:O-M23-3 TLH43085                        INJT.  TIME -   02:55
1004

  80J
  40:.

  20.
   0.
                                                            A5.}.
                                                                4E6
                 19:00            20:00            21:00            22:00
 File:S97586S #1-905 Acq:13-SEP-1997  02:52:21 EI+ Voltage SIR 70S Noi»e:76
 317.9389 T:2 BSUB(256r 30, -3. 0) PKD(9, 5,5, 0. 05\,304. 0,1. 00*,JT, T) Exp:EPCUS
 TRJANGLE LABS  Teit:O-M23-3 Ttl#43085                       JMT. TIME -   02:55
 1001                                                       A6.92E6

  sol

  50J

  401

  20.

   0:
                                                                                     23:00
1.5X6

1.2X6

9. OE5

6.0E5

3. 0X5

O.OEO
   Tim



.2.0E6

.1.6E6

.1.2X6

.8.1E5

.4.1ES
                  19:00            20:00           21:00            22:00
 File:S975868 #1-905 Acq:13-SEP-1997 02:52:21 EI+ Voltage SIR 70S
 330.9792 T:2 Exp:EPCUS
 TRIANGLE LABS  Text:O-M23-3  TLIt43085                       INJ. TIME  -
                                                                                     23:00
                                                                                                      .O.OEO
                                                                                                          Tim.
                                                                             02:55
                  19:00            20:00           21:00
 rile:S975868 #1-905 Acq:13-SEP-1997 02:52:21 SI+ Voltage SIR 70S
 375.8364 T:2 Exp:EPCOS
 TRIANGLE LABS  Text:O-M23-3  TLH43085
 100J
                                                                    22:00
                                                               IKJ.  TIME
                                                                                     23:00
                                                                             02:55
   401

   201

    0.
                                                                                             23 29
      18:16
                                   19:59
                                                                                                j\—L
                  19100
                                   20100
.O.OEO
    Tim
.1.1X4

.8.8X3

i6.6E3

.4.4X3

.2.2X3
                                                    21100
                                                                    22100
                                                                                     23100
                                                                                                       .0.0X0
                                                                                                           Tim
                                                                                                           130

-------
\rll»:S975868 tl-905 Aoqtl3-SSP-1997 03i53t31 Eli- Voltage SIX 70S Nolle:56
319.6965 F:2 BSUB(256, 30, -3.0) PKD( 7,5, 3, 0.05\,234.0,1.00\,r,T)  ExptEPCUS
TXIAKGLX LABS  TuxttO-K33-3 TLH4308S                        HKT. TIM* -   03i55
100*
                                                                                                   0.9*9
            20:00                 21:00                23:00                23:00
 riletS975a68  tl-905 Acqtl3-SEP-1997  02:52:31 EI+ Voltage SIS 70S Holm* t 72
 321.8936 f>2  BSUB(256, 30, -3.0) PKD(7, 5,3, 0 .OS\, 288.0, 1.00\,r,T) ExptEPCOS
 TX1ANSLE LABS  T*xttO-M33-3 TLH43085                       IXT. TIME -   03*55

 100J
  so:
  60:
          A5.
  40.
  20:
            20:00                21:00                22:00                 23:00
rile:S975868 tl-905 Acq:13-SEP-1997 03:53:31 EI+ Voltage SIX 70S No±me:422
331.9368 T:2 BSUB(356,30,-3.0)  PKD(7,5,3, 0.05\,1688.0,1.00\,r,T) ExpsEPCUS
TRIANGLE LABS  Text:0-M23-3  TLIt43085                       HKT. TIME  -   02:55
                                                         A3.65E6
                                                            ..A3.57E6
 60:
 40:
 20:
               -r
                                    T
                                                                               rr
            20s00                 21:00                22:00                23:00
rile:S975868  tl-905 Aojsl3-SEP-1997 02:52:21 EH-  Voltage SIX 70S No±ae:144
333.9338 T:2  BSUB(356,30,-3.0) PKD(7, 5,3,0.05\,576.0,1.00\,r,T)  ExpsEPCUS
TRIANGLE LABS  Text:O-M23-3 TLIt43085                        UKT. TIME "   02:55
1001
  80:
  60:
  40:
  20:
                                                            II,,
                                                                /	V
              20:00                21:00                22:00                 23:00
  rlle:S975868 tl-905 Aoqs13-SEP-1997 02:52:21 EH- Voltage SIX 70S Noise:188
  327.8847 F:2 BSUB( 256, 30, -3 . 0)  PJO)( 7, 5, 3, 0. 05%, 752. 0, 1. 00\,T, T) Exp:EPCUS
  TRIANGLE LABS  TextsO-M23-3  TLH43085                       IXJ. TIME  -    02:55
  1004                                                         A6.96E6
   80:
   60:
   40:
   20.
              20:00                21:00                 22>00                23:00
  rile:S975868  tl-905 Acq:13-SEP-1997 02:52:21 EI+  Voltage  SIX 70S
  330.9792 P:3  ExptEPCUS
  TXIANGLE LABS  Text:O-M23-3 TLIt43085                        IKT.  TIME -   02:55
                               20:4821:03   ->T .«     2ii-54    22i17   — - '- •22-5fi
              30 > 00
                                    21:00
                                                         22:00
                                                                              331 00
                                                                                                  .1.1E6
                                                                                                  -9.1E5
                                                                                                  16.8E5
                                                                                                  L4.6E5
                                                                                                   O.OEO
                                                                                                      Time
                                                                                                   .1. 3E6
                                                                                                   .1. 1E6
                                                                                                   .8.115
                                                                                                   .5.4E5
                                                                                                   .2.7E5
                                                                                                   .O.OEO
                                                                                                       Time
                                                                                                   2. ore
                                                                                                  .1. 6E6
                                                                                                  .1.2E6
                                                                                                  '-.7.9E5
                                                                                                  .4.0ES
                                                                                                    .O.OEO
                                                                                                       Time
                                                                                                            13

-------
 lle,S975868 tl-905 Aoq,13-SEP-1997  02:52,21  11+ Voltage SIX 70S Hoiae:80
 39.8597 T:2 BSOB(256,30, -3.0) PXD(7,5,3, 0.05%, 330.0,1.00\,r,T) Xxp,XPCUS
TXIAHSLX LABS  TexttO-M23-3 TLH43085                        OU. TIM* -   02»55
              24iOO                 25iOO                 20iOO
FllesS975868 tl-905 Acq,13-SEP-1997 02:52:21 EI+ Voltage SIX 70S Hoifet68
 41.8567 T:2 BSUB(256,30,-3.0) PKD(7,S,3,0.05\,373.0,1.00\rF,T) Exp:EPCUS
TXIAXCUS LASS  TexttO-M23-3  TLH43085                       ISJ. TIMX -    03:55
      A4.24X4
                                                                                27tOO
              24:00                 25:00                 26:00
rile:S97586B  #1-905 Acq:13-SEP-1997 02:52:21 EI+ Voltage SIX 70S Koiae:61
351.9000 Fi2  BSUB(256,30,-3.0)  PKS(7,5,3,0.05\,244.0,1.00\,F,T) Xip:EPCUS
TRIANGLE LABS  Text:O-M23-3 TLIt43085                       JK7. TIME  -    02:55
100*                                                             A4.S4E6
                                                  A4.83E6
  so:
  60:
  40:
  20:
   o\	.	L
                                                                                27-00
                ~r
                                      ~r
              24:00                 25:00                 26:00
Flle:S975868  tl-905 Acq:13-SEP-1997 02:52:21 EI+ Voltage SIX  70S Hoiae:63
353.8970 F:2  BSUB(256, 30, -3. 0) PKD( 7, 5, 3, 0. 05\,252. 0,1. 00%, T, T) ExpsEPCUS
TXIAKGLE LABS  Text:O-M23-3 TLI#43085                       ISJ-. TIME -   02:55
                                                                                2700
 1003
  SO:
  60:
  40:
  20:
   0.
                                                  A3.
                                                     56E6
                                                                  A3 . 05E6
              24:00                 25:00                 26:00
 rile:S975868 tl-905 Acq:13-SEP-1997  02:52:21 EI+  Voltage SIS 70S
 330.9792 F:2 ExpiEPCUS
 TRIANGLE LABS  Text:O-M23-3 TLIt43085                        HTJ. TIME -
 10<>3i          24:01             24:49     25:17 25:34             26:22
     .  ^^  /^«-\
  ao3
  eol
  40:
  20:
   o:
                                                                                 27  00
                                                                            02:55
                                                                                    27:09
                T
                                      rr
                                                            -r
               24:00                 25:00                 26:00
 File:S975868 tl-905 Acq:13-SEP-1997 02:52:21  SI+ Voltage SIX 70S
 409.7974 F:2 Exp:EPCUS
 TRIANGLE LABS  Text,O-M33-3  TLH43085                       IKT. TIMX -
 1001
                                                                                 27«00
                                                                            02i55
  80:
  60:
  40:
  20:
   0.
           23:50
                     24:10
                             24:38
                                         3Stii
 25:52
JLJL
               24:00
                                     25:00
                                                                  26:19
                                                                 ^»^>A__A.
                                                                                    27:09
                                                           26\00
                                                                                 27iOO
                                                                                                      1.4E6
                                                                                                      1. 0X6
                                                                                                      .6.9X5
                                                                                                      .3.4X5
                                                                                                      .0.0X0
                                               1.3X6
                                               9.3X5
                                               7.0X5
                                               4.7X5
                                               2.3X5
                                               .0.0X0
                                                   Tim
                                                                                               27:38
                                                                                                       8.3X6
                                                                                                       6.6X6
                                                                                                       5.0X6
                                                                                                       3.3X6
                                                                                                      .1. 7X6
                                                                                                       O.OEO
.1.5X4
-1.2X4
-8.8X3
.5.9X3
.2.9X3
 0.0X0
                                                                                                          132

-------
r±J.e,SS75868 H-905 AcqilJ-sSP-1997 OliSiill XI+  Volttym SIM 70S Ho±tet65
355.8546 Tt2 BSC3(256,30,-3.0) PKD(7,5,3,0.05\,260.0,1.00\,r,T) XxptXPCUS
TRIANGLE LABS  TmxtiO-M23-3 TLH43085                        XK7. JTMT -   02t55
   24,48  25:00  25,12 25,24 25,36  25,48  26,00 26,12 26134 26,36  26,48 27:00 27,12 27,24  27,36
r±le:S975868 «1-905 Aoqtl3-SXf-1997 02,52,21 XI* Voltmge SIS 70S Ho±me:54
357.8516 T>2 BSUB(256,30,-3.0)  PXD(7,5,3,0.05\,216.0,1.00\rr,T) ExpiXPCUS
TRIANGLE LABS   Tejct,O-M23-3 TLH4308S                       OUT. TIME -    02tSS
100*
                             A3.39E3
  80j

                                                                            A7.64E3
                                                                                      A6.13E3
                                                                                                -8.1X3

                                                                                                .6.5X3

                                                                                                '-4.9X3

                                                                                                .3.3X3

                                                                                                '.1. 6X3

                                                                                                 0.0X0
   24:48 25:00  25:12  25,24 25:36 25:48 26:00  26:12 26:24 26:36 26:48  27:00 27:12 27:24 27:36
rile:S97S868 il-905 Acq,13-SEP-1997  02,52:21 EH-  Voltage SIX 70S No±ae:62
367.8949 Tt2 BSUB(256,30,-3.0) PKD(7,5,3, 0. 05\,248. 0,1. 00\,T, T) XxptEPCUS
TRIANGLE LABS   Text:O-M23-3  TLI#43085                        JWJ. TIME -   02:55
1001                                                          A3.Q8E6

 so:

 tfo:

 40:
                                                                                                     Time
  20:
                                                                     \2.44E5
                                                                       A	
                                                                                                 '.9.1X5

                                                                                                 L6.9E5

                                                                                                 .4.6E5

                                                                                                 -2.3E5
                                                                                                  .O.OEO
    24:48 25,00  25,12 25:24 25:36  25:48  26:00 26:12 26:24 26,36  26:48 27:00 27:12 27:24  27:36
 T±le:S975B68 fl-905 Aoq:13-SEP-1997 02:52:21 EI+ Voltage SIX 70S Noiae:59
 369.8919 T:2 BSUB(256, 30, -3 . 0)  PKD(7,5,3, 0.05\,236. 0,1. 00\,T, T) ExptEPCUS
 TXIAKGLE LABS   Text:0-M23-3  TLI#43085                       JKT. TIME -   02,55
                                                                                                      Tine
  100*
   80.
   60:
   401
   20:
                                                                A2.
                                                                                                .-7.8E5
                                                                                                  .6.2X5
                                                                                                  .4.7X5
                                                                                                  '.3. 1X5
                                                                                                  11. 6X5
                                                                     SI. 65E5
                                                                       A	
                                                                                                  .O.OEO
     24,48 25:00 25,12  25,24 25:36 25:48 26:00 26:12  26:24  26:36 26,48 27:00  27:12 27:24 27:36
  rile:S975868 41-905 Acqtl3-SEP-1997 02:52:21 EI+ Voltage SIX  70S
  330.9792 T:2 XxptXPCOS
  TXIANGLE LABS  Text:O-M23-3 TLIt43085                       XKJ. TIME -   03:55
                                                                                                      Time
  1003

   BO.


   60.

   40.

   20.
                   25:17
                            25:34    25:50
 8.3X6

'.6.6X6

.5.0X6

.3.3X6

.1. 7X6

.O.OEO
     24:4825:25i2 25s24 2S36
                                                                    26 1 48  27:00 27:12 27:24  27:36
                                                                                                      Tim^
                                                                                                            13

-------
rilatS975868 tl-346 Aoq,13-SXP-1997 02,52,21 XI + Voltaym SIX 70S Holm*, 454
373.8208 f,3 BSUB(256,30, -3.0) PKD(7,5,3,0
TRIANGLE LABS T«xt:O-At23-3 2X1*43085
100]
80:
50:
40:
20.





05%, I8is.o,i.oo%,r, r; xxptxpcos





A1.66E4 A1.04X4 A1.59E4 Al.

J**^- - rt~i A ~\-***
IHJ-. TIME - 02:55
_7.4Jf4



8714 A7.75X3 . , ,
8'X4 j A6.13XJ

.5.5X4
.4.4X4
.3.0X4
.1.5X4
.0.0X0
28:12 28:24 28:35 28:48 25.66 25:12 25:24 25:35 25:48 30:66 30:12 30:24 30:35 30:48 31:00 TlM*
rile:S975868 tl-346 Acq,13-SEP-1997 02,52,21 EH- Voltage SIX 70S Noil* i 327
375.8178 r,3 BSUB(256,30, -3. 0) PXD(7, 5,3,0
TRIANGLE LABS Teit:0-M23-3 TLIt43085
100]
80:
so:
40J
20:
o:






.05\,1308.0,1.00\,r,T) Elp:XPCUS







IKJ-. TIME - 02,55
-1 . 8X5





.1.4X5
.1.1X5
.7.1X4
.3.6X4
O.OEO
28:12 28:24 28:35 28:48 25:66 25:12 25:24 25:35 25:48 30:66 30:12 30:24 30:35 30:48 31:00 Time
Tile:S975868 tl-346 Acq:13-SEP-1997 02:52:21 EI+ Voltage SIR 70S Noisa,295
383.8639 f:3 BSOB(256,30, -3 .0) PKD(7,5,3,0
TRIANGLE LABS Text:O-M23-3 TLIt43085
100]
80:
;
so:
40:
20J
0:.
A2
A



1
i y \
.05\,1180.0,1.00\,r,T) ElpiEPCUS

I7*6 Al.





i \ y
IITJ-. TIME - 02:55
8SE6
1
A1.46E6
A


i y i
-8.1E5
'_6.5ES

-4.9E5
.3.2X5
-.1 . 6E5
0 . OEO
28:12 28:24 28:35 28:48 25:66 25:12 25:24 25:35 25:48 30.'66 30:12 30:24 36:35 ' 30:48 ' 31: 00 Tiae
Tile:S975868 tl-346 Acq:13-SEP-1997 02:52:21 EI+ Voltage SIR 70S Noiae:455
385.8610 F:3 BSUB(256,30,-3 .0) PKD(7,5,3,0 .OS\,1820 .0,1.00\,r,T) Exp:EPCUS
TRIANGLE LABS Text:0-M23-3 TLIf430S5
1003
80:
so:
40:
20:
o:

A4.33E6




J
28:12 28:24 28:35 28:48 25:66 25:
rile:S975868 tl-346 Acq:13-SEP-1997 02:52
392.9760 T:3 Exp:EPCVS
TRIANGLE LABS Tejct,O-H23-3 TX.H43085
1004
80:
so:
40J
20:
o:
A3



J l y
IJCJ. TIME * 02:55
,_! . 7E6
66E6
\ A2.83E6
A
A

I y i
:l . 4E6
.1 . OE6
.6.9E5
.3 . 4E5
O.OfO
12 25:24 25:35 25:48 30:00 30:12 30:24 30:35 30:48 31:00 Time
21 EI+ Voltage SIR 70S



^^^nY^/YN^n^^nVvvXpAV^




^^V\r v\yv» '





UTjr. TIME - 02:55
29:56 30:11 ,0.2B 30:47 _4.3SS
'Wyx^/v\/v>^/\ /^^JYVvflTV
\jf



.3.4E6
.2.6E6
.1 . 7X6
.8.6B5
O.OEO
28:12 28:24 28:35 28:48 25166 25:12 25:24 25:35 25:48 30:66 30:12 30:24 ' 30:35 ' 30:48 ' 31:00 Time
rile:S975868 tl-346 Acq:13-SEP-1997 02:52:21 EI+ Voltage SIR 70S
445.7555 T:3 Exp:EPCUS
TRIANGLE LABS Te*t:0-M23-3 TLJ*43085
100]
80J
60:

40:

20:
o:



28:58
1
I
21" aa&"i4l M.,a9{°
U* — ^JvV^^^^_^O\^^-^AA^AA^^;vVA
-------
nio:SS75B68 #1-346 AcqilJ-SXP-1997  02:52:11 SI+ Voltmg* SIM 70S Hoif9t235
389.8156 Ts3 BSUB(256,30,-3.0) PKD(7,5,3,0.05\,940.0,1.00\,P,T) XxpifPCUS
TXIANGLX LASS  T»Xt:O-M23-3 TLIH3085                       I1KT. TIM* -   03.55
1001                                              A4. 5X3
     38:36   28:48   29:00    29:12   29:24    29:36   29:48    30:00   30:12    30:24   30:36
rile:S975868  #1-346 Acq:13-SEP-1997 02:52:21 EI+ Voltage SIX  70S Hoif»:434
391.8127  T:3  BSUB(256,30, -3. 0)  PKD(7,5,3, 0. 05\,1736.0,1.00\,T, T) ExpiEPCUS
TRIANGLE  LABS  Teit:O-M23-3  TLH43085                       IKJ. TIME  -   02:55
1001
                                                                                                 .9.3X3
     28:36   28:48    29:00   29:12    29:24   29:36    29:48   30:00    30:12
 rile:S975868 #1-346 Acq:13-SEP-1997  02:52:21  EI+  Voltage SIS 70S Hoi.ee-.444
 401.8558 F:3 BSUB(256,30, -3. 0) PKD(7,5,3, 0. 05\,1776. 0,1. 00\,T, T) Exp:EPCUS
 TRIANGLE LABS  Text:0-M23-3 TLI#43085                        INJ. TIME -   02:55
 1001                                                                     A2.07E6
                                                              A2.63E6

  ao:

  60:

  40.

  so:
                                                                                 30:24
                                                                          30:36
 O.OEO
    Time



.1.1E6

.9.0ES

 6.7E5

 4.5E5

 2.2E5

 O.OEO
     28:36    28:48   29:00    29:12   29:24    29:36   29:48    30:00    30:12    30:24   30:36
 rile:S975868 #1-346 Acq:13-SEP-1997 02:52:21 EH- Voltage SIR 70S N6iae:293
 403.8529 T:3 BSDB(256,30, -3. 0)  PKD(7,5,3, 0. 05\,1172. 0,1. 00\,T,T) Exp:EPCUS
 TRIANGLE LABS  Text:O-M23-3  TLI#43085                       IJKT. TIME -   02:55
 10 OS,
  00J
  so:
   40.
   20:
                                                              A2.16E6
                                                                           A2.,
                                                                                   9.2E5

                                                                                   7.3E5

                                                                                   .5.5E5

                                                                                   .3. 7E5

                                                                                   .1. 8E5

                                                                                   O.OEO
      28:36   28:48    29:00   29:12    29:24   29:36    29:48   30:00
 File:S975868 #1-346 Acq:13-SEP-1997 02:52:21 EH-  Voltage SIS 70S
 392.9760  T:3 Ezp:EPCOS
 TRIANGLE  LABS  Text:0-M23-3 TLI#43085                        IKT.  TIME -
                                                                         30:12
                                                                                  30:24
                                                                                           30:36
                                                             02:55
  1001

   80.

   60.

   40.

   20.
28:SO.i 39101
                   29,16
                                            47
                                                              29:56
                                                                         30:11
                                                                      30:2t
 .4.3E6

 .3.4E6

 .2.6E6

 11.7E6

 .8.6X5
      28:36
               28:48
                       29:00
                                29:12
                                        29:24
                                                 29:36   29:48
                                                                 30:00
                                                                          30:12
                                                                                  30:24
                                                                                           30:36
                                                                                                    O.OEO
                                                                                                       T±mi

-------
 'ilm,S975868 tl-390 Acq,13-SEP-1997  03tS2t2i £1+ Voltage SIX 70S Holme,869
407.7818 T>4 BSU*(256,30,-3.0) tKD(7,5,3,0.05\,3476.0,l.OO\,T,T) KxptXPCUS
TSIAXGLX LAM  Text,O-M23-3 TUH3085                        IHJ. TIM* -   02tS5
1004   A7  62X4
     31,48     32:00      32', 12     32', 24      32', 36     32:48      33', 00
rile,S97S868 tl-390 Aoqil3-SEP-1997 02,52,21 XI+ Voltage SIS 70S HOime:477
409.7789 f:4 BSUB(256, 30, -3. 0) PKD( 7,5, 3, 0.05\, 1908.0,1.00\,f,T) ElptEPCUS
TSIANGLX LABS  TeittO-M23-3 TLIt43085                       1X7. TIME -   02:55
1004                   A1.91E4
     31:46      32,00      32', 12      32:24     32:36      32:48
rile,S975868  tl-390 Acq,13-SEP-1997 02:52,21 EI+ Voltage SIS 70S
417.8253 f,4  BSUB(256, 30, -3. 0)  PKD( 7,5, 3, 0.05\,1988. 0,1 . 00\,T, T)
TSIANGLE LABS  Text:O-M23-3  TLH43085                       JWT.
                                                                              33,12
                                                                                         33124
1003

  80:

  60:

  40:

  20:

   0.
            A9.Q8E5
                                                                    33:00     33,12
                                                                  Soiae,497
                                                                  Exp:EPCUS
                                                                  TIME  -  02:55
                                                                          A6.11ES
                                                                                         33:24
                                                 ~r
                                                           -r
     31:48      32:00     32:12      32:24     32:36      32:48
rile:S97S868  tl-390  Aoj,13-SEP-1997 02,52:21 EI+ Voltage SIR  70S
419.8220 F,4  BSUB(256,30,-3.0)  PKD(7,5,3,0.OS\,3164.0,1.00\,T,T)
TRIANGLE LABS  Text:O-M23-3 TLIt43085                       XK7.
10OS        A2.09E6

  80:

  60:

  40:

  20:

   o:
                                                                      -r
                                                                    33:00
                                                                  HOi*e>791
                                                                  Exp:EPCUS
                                                                  TIME -   02s55
                                                                          A1.39E6
                                                                               i* I  i  i  i 1 i  I^P  i 'i  i" i
                                                                              33:12      33:24
                                      ~r
                                                 rr
     31:48      32:00      32:12      32:24      32:36     32':48
rile:S975868 tl-390 Acq:13-SEP-1997 02:52:21 XI+ Voltage SIS 70S
430.9729 T:4 ExpsEPCUS
TRIANGLE LABS   T&rt,O-M23-3  TLIt43085                       TJCJ.
      31:49  31,
 80:

 60:

 40:

 20:

  o:
                                                                    33:00
                                                                               3312
 i i  i  i  r i  i
33:24
             .3. 8X5

             .3. 0X5

             .2.3X5

             .1.5X5

             .7.6X4

             .0.0X0
                Time



             .8.3X5

             .6.6X5

             .5.0X5

             .3.3X5

             .1. 7X5
                                                                   TIME -   02:55

                                                                   3258   33:06
        .'Vfl' '  ' 32\00'  ' '  32\12' '  ' 32\24 '  '  ' 32\36 '  '  '32:48' '
 r±le:S97586S tl-390 Acq:13-SEP-1997 02:52:21  EI+ Voltage SIS 70S
 479.7165 F:4 XzptEPCUS
 TRIANGLE LABS  Teit:0-M23-3 TLIt43085                        UTJ.
                                                                               i  I i  i  i  i  i I  i  i  i—i—r
                                                                              33:12      33:24
                                                                                                      0.0X0
                                                                                                         Time
                                                                                                      .3 . OE6

                                                                                                      .2.4E6

                                                                                                      .1 . 8X6

                                                                                                      .1.2X6

                                                                                                      .6.0E5
                                                                                                      .0.0X0
                                                                                                          Tim
                                                                   TIME -   02: 55
                                                                     33,00      33:12      33:24
      31:48
                32:00
                           32:12
                                     32:24
                                                32,36
                                                          32:48
                                                                                                          Time
                                                                                                            131

-------
 23.7766 Tt4 BSUB(256,30,-3.0) PKD(7,5,3,0.OS\,1592.0,1.00\,T,T) Exp:EPCUS
TRIANGLE LABS  TvftiO-M23-3 TLH43085                        IKT. TIM* -   03i53
                                                                                                    0*9
  32:00  32i06  32>12   32tl8  32,24  32t30  32:36  32:42  32:48   32:54  33:00
ile:S975868 fl-390 Acqtl3-SEP-1997  02:52:21 EH- Voltag* SIX 703 Noil*: 213
25.7737 T:4 BSUB(256, 30, -3.0) PKD( 7,5, 3, 0. 05\, 852.0, 1.00\,T,T)  Exp:EPCOS
 IASSLE LABS  Tmit:0-M23-3 TLH43085                        HKT. TIMS -   02:55
                                                                                    33:06  33:12
                                                                                                  O.OEO
   32:00   32:06   32:12  32:18   32:24   32:30  32:36   32:42  32:48  32:54   33:00
r±la:S975868  tl-390 Acq:13-SEP-1997 02:52:21 EH- Voltage SIX 70S Koiae:484
 35.8169 r:4  BSOB(256,30, -3.0)  PKD(7,5,3,0.05\,1936.0,1.00\,T,T) Exp:EPCUS
TXIANGLE LABS T*xt:O-M23-3 TLI»43085                       TJW. TIME  -   02:55
100^                                                      A1.39E6
  eo:

  40:

  20.
                                                                                   33:06  33:12
                                                                                                    Time
    32:00   32:06  32:12  32:18   32:24  32:30   32:36  32:42  32:48   32:54   33:00
 r±lesS975868 H-390 Aoq:13-SEP-1997 02:52:21 EH-  Voltage SIX  70S Hoiae:230
 437.8140 F:4 BSUB(256,30,-3.0) PKD( 7,5,3, 0. 05%, 920. 0,1.00\,f, T)  ExpsEPCUS
 TRIANGLE LABS  Text:O-M23-3 TLI*43085                       INJ. TIME -   02:55
 1001                                                      A1.33E6
  so:

  so:

  
-------
 ile:S975B68 tl-390 Aoqil3-SXP-1997 02:52:31 11+ Voltfym SIX  70S Noilfi382
 41.7428 rt4 BSU*(256,30,-3.0)  PKD(7,5,3,0.05\,1528.0,1.00\,F,T) XxptXPCUS
TXIANGLX LABS  T*xt:O-M23-3 TLH430B5                       IXT. TIM*  -   02>55
 on
 SOI
 801
 701
 sol
 50.
 40.
 30.
                    32>00               33i00               34:00
Til*tS975868  tl-390 Acq:13-SEP-1997 02iS2>21 EH- Voltage  SIX 70S Koit»,354
 43.7399 Ti4  BSUB(256,30, -3. 0) PKD(7,S,3, 0. 05\, 1416. 0,1.00\,T, I) Xxp:XPCUS
TRIANGLE LABS
1001
     A1.57S4
                                                            A2.03S4
                                                                                       A1.54E4
                                                                               35:00
.3.8X4
.2.5X4
.2.2X4
.2.0X4
ll. 7X4
11.4X4
.1.1X4
.8.4X3
.5.6X3
.2.8X3
-.0.0X0
    T±me
                Text:0-M23-3 TLIt43085
                                                              INJ-.  TIME -   02:55
                     32:00               33:00               34:00
 rile:S975868 tl-390 Acq:13-SXP-1997 02:52:21  EI+ Voltage SIX 70S
 430.9729 T:4 ExpiEPCUS
 TRIANGLE LABS  T*xt:O-H23-3  TLIt43085                       IJW. TIME
                                                                                35:00
1003

 sol
 701
 601
 sol
 40.
 30.
 20.
 10.
  0.
              31139
                          32:16
                                                                                                 35:51
                     32:00               33:00              34:00               35:00
 rile:S975868 tl-390 Acq:13-SEP-1997 02:52:21 EI+ Voltage SIX  70S
 513.6775 T:4 ExptEPCUS
 TRIANGLE LABS   TejcttO-M23-3 TLH43085                       JWJ.  TIMX "   02i55
                                       32 55
 .3.0X6
 .2. 7X6
 L2.4E6
 12.1X6
 .1. 8X6
 .1.5X6
 .1.2X6
 .9. 1X5
 .6.1X5
 13. 0X5
  0.0X0
     Tim
                     32tOO
                                         33:00
                                                             34:00
                                                                                35,00
                                                                                                        138

-------
 '±le:S975BS8 U-390 Acqtl3-SgP-1997 02:S2t2i xH- Voltmgt SIS  703 Holme,2B6	
 57.7377 Tt4 BSUB(256,30,-3.0)  PKD(7,5,3,0.05%,1144.0,1.00%,r,T) XxpiEPCOS
TRIANGLE LASS  Text,O-M23-3  TLIH3085                       IJKT. TIM* -   03.55
 00\
             35tl2         35', 18         35', 24         35', 30         35', 36
 ileiS975868 #1-390 Acqil3-SEP-1997 02:52,21 II* Volttgm SIM 70S Noimetlll
 59.7348 Ts4 BSUB(256,30,-3.0)  PKD(7,5,3,0.05\,444.0,1.00\,T,T)  ExpiEPCUS
TRIANGLE LABS   Text,O-M23-3 TLI#43085                        UKT. TIMS -   02»55
 00*                             A2.44E4
      35143
              35sl2         35:18        35:24         35:30         35i36
 •±le:S975868 tl-390 Acg:13-SEP-1997  02:52:21 EI+  Voltage SIX 70S lK>iae:153
  69.7779 T:4 BSUS(256,30,-3.0) PXD(7,5,3,0.05\,612.0,1.00\,T,T) ExpsEPCOS
 TRIANGLE LABS  Text:O-M23-3 TLH43085                        IKJ. TIME -   02i55
  003,                          A8.J
  80.

  60.

  401

  20.
      35:42
                -r
                                                         T
              35.-1.2         351-18         35:24         35:30         35i36
 riletS975868 #1-390 Acq»13-SEP-1997 02iS2i21 SI+ Voltage SIR  70S Noiae>44
 471.7750 T:4 BSUB(256,30f-3.0)  PXD(7,5,3,0.05\,176.0,1.00\,T,T) ExptEPCUS
 TRIANGLE LABS  Text.-O-M2.3-J  TLI043085                       INJ. TIME -   02:55
 1001                           A8.?BE5

  80.

  60.

  40:

  20.
      35:42
              35:12         35il8         35:24         35:30         35s36
 rile:S975868 11-390 Acqil3-SEP-1997 02:52:21 EI+ Voltage  SIR 70S
 430.9729 T:4 ExpsEPCUS
 TRIANGLE LABS   Text:O-M23-3 TLH43085                        UKT. TIME -
 100*                                   35,23                       35:35
   00J

   60.

   40.

   20.
       35:42
02:55
               35,12
                             35>ia
.O.OEO
    Time
                      2.8E5

                      2.3E5

                      .1. 7E5

                      .1.1E5

                      .5. 7E4
                     .O.OEO
                         T±m
                      3.715

                      2.9E5

                     .2.2E5

                     .1. 5E5

                     .7.4E4
                                           35,24
                                                                      35:36
                                                                                    35:42
                      .O.OEO
                         Tim
                      3.0E6

                      2.4X6

                      1. 8E6

                      .1.2X6

                      .5.9X5


                      .0.0X0
                          Tim

-------
'ile:S975868  #1-346  Acq:13-SEP-1997 02:52:21 EI+ Voltage SIR 70S
73.8208  F:3  Exp:EPCUS
lample Text:O-M23-3  TLI#43085                       INJ.  TIME =
LOOi
              02:55 File Text:O-M23-3 TLI#4»
                30 22                _1.0E4
                           29:00                        30:00
ile:S975868 #1-346 Acq:13-SEP-1997  02:52:21  EI+ Voltage SIR  70S
75.8178 F:3 Exp:EPCUS
ample Text:O-M23-3 TLI#43085
.00%
INJ. TIME =
                                     O.OEO
                                        Time
02:55 File Text:0-M23-3  TLI#4»
                      _7.0E3
            30:45
                      L5.6E3
                           29:00                        30:00
ile:S975868 #1-346 Acq:13-SEP-1997 02:52:21 EI+ Voltage SIR 70S
83.8639 F:3 Exp:EPCUS
ample Text:0-M23-3 TLI#43085                       INJ. TIME =
                                oo ??X17         29:46
                                        Time
              02:55  File Text:0-M23-3 TLI#4»
80 1
60 j
40 1
20J
o"
f'J • •LJ-/\ A
(1 "A

u A /
29

V
29:00 30:00
L6.5E5
L4.9E5
13.2E5
L1.6E5
: O.OEO
Time

-------
TLI Project:      43085
Client Sample:   O-M23-FB
Method 23 PCDD/PCDF Analysis (a)
             Analysis File:  S975833
Client Project:
Sample Matrix:
TLI ID:

Sample Size:
Dry Weight:
GC Column:
S413-004
M23Train
181-55-4ABD

1.000
n/a
DB-5

Date Received:
Date Extracted:
Date Analyzed:
Dilution Factor:
Blank File:
Analyst:

09/03/97
09/04/97
09/11/97
n/a
S975815
BJG

Spike File:
ICal:
ConCal:
% Moisture:
% Lipid:
% Solids:

SPX23704
SF56117
S975814
n/a
n/a
n/a
Amlytesw:-:
2,3,7,8-TCDD
1,2,3,7,8-PeCDD
1,2,3,4,7,8-HxCDD

1,2,3,6,7,8-HxCDD
1,2,3,7,8,9-HxCDD
1,2,3,4.6,7,8-HpCDD
1,2,3,4,6,7,8,9-OCDD
2,3,7,8-TCDF
1,2,3,7,8-PeCDF
2,3,4,7,8-PeCDF
1,2,3,4,7,8-HxCDF
1,2,3,6,7,8-HxCDF
2,3,4,6,7,8-HxCDF
1,2,3,7,8,9-HxCDF
1,2,3,4,6,7,8-HpCDF
1,2,3,4,7,8,9-HpCDF
1,2,3,4,6,7,8,9-OCDF

totals v:;:.'";;: •'• :'^.,X
Total TCDD
Total PeCDD
Total HxCDD
Total HpCDD
Total TCDF
Total PeCDF
Total HxCDF
Total HpCDF
Amt. (ng) Dt EMPC
EMPC 0.009
0.04
0.02

0.03
0.03
0.03
0.09
0.02
0.04
0.04
0.03
0.03
0.03
0.03
EMPC 0.03
0.02
0.03

'•^f^cJ^Anit'tng) Number Dt EMPQ
EMPC 0.009
0.04 1
0.09 3
0.04 2
0.02 1 0.02
0.08 2 0.09
0.11 4
0.02 1 0.05
Ratio

1.67
1.39

1.22
1.23
0.94
0.94
0.70
1.66
1.36
1.43
1.14
1.17
1.08

1.03
0.88










*T

25:51
29:08

29:13
29:30
32:04
34:38
20:23
24:43
25:29
28:22
28:29
29:00
29:42

32:25
34:44










**Bi*i-' '


o
v<—


B_
B_
B_






B_

B_

Flags



—




                                        Page 1 of 2
                           X237.PSR vlOO. LARS 6.10.0.
 Triangle Laboratories, Inc.®
 801 Capitals Drive • Durham, North Carolina 27713
 Phone: (919) 544-5729 • Fax: (919) 544-5491
                       Printed: 14:06 09/1 i

-------
TLI Project:      43085
Client Sample:   O-M23-FB
           Method 23 PCDD/PCDF Analysis (a)
                       Analysis File:   S975833
Internal Standards
13C,2-2,3,7,8-TCDF
13C12-2,3,7,8-TCDD
13C,:-l,2,3,7,8-PeCDF
13C,2-l,2,3,7,8-PeCDD
13Ci2-l,2,3,6,7,8-HxCDF
13Ci2-l,2,3,6,7,8-HxCDD
13Ci2-l,2,3,4,6,7,8-HpCDF
13C,2-l,2,3,4,6,7,8-HpCDD
13Cr-l,2,3,4,6,7,8,9-OCDD

Surrogate Standards (Type A)
37CL,-2,3,7,8-TCDD
13C12-2,3,4,7,8-PeCDF
13Ci2-l,2,3,4,7,8-HxCDF
13C,2-l,2,3,4,7,8-HxCDD
13Ci2-l,2,3,4,7,8,9-HpCDF
•Alternate Standards (Type A)
13C,2-l,2,3,7,8,9-HxCDF
'3Cp-2,3,4,6,7,8-HxCDF

Recovery Standards
13C,2-1,2,3,4-TCDD
13C12-l,2,3,7,8,9-HxCDD
AmL (ng)
3.0
2.9
3.0
3.5
3.3
3.1
3.0
3.5
7.0

%trlN}
3.8
3.6
33
2.9
2.7
Amt (n§)
2.8
33



%R«*very
75.7
71.5
75.4
86.9
81 3
76.5
75.9
87.9
876

% Recovery
95.6
89.4
83 1
72.6
67.8
% Recover^
69.7
81 5

V

QC Limits
40%- 130%
40%-130%
40%- 130%
40%- 130%
40%-130%
40%- 130%
25%-130%
25%-130%
25%- 130%

:VQC Limits^ :';.-::"
70%- 140%
70%- 140%
70%- 140%
70%- 140%
70%- 140%
FQOtiRiltS:'^:
40%- 130%
40%- 130%

: :f\ .,;.

Ratio
0.77
0.80
1.55
1.49
050
1.21
0.42
0.99
086

^•Rallo?:^.
1.59
051
1.23
0.42
t:-R»*
0.49
0 50

^•Ratio:-:^
0.81
1.21
RT
20:22
21:12
24:42
25:51
28-28
29:12
31-11
32:04
34-37

Strr-,,
21:13
25:28
28-21
29:07
32:25
:£ffnr:-V
29:41

-!«?r-
20:59
29:29
Flags
—
—
—

Flags
—
oIL
v 	
:.?-Ffci>gs";;-:'
	

*J$*i&:::
—
                     Data Reviewer.
2LJ.
                                        Page 2 of 2
09/18/97
                                                                          X237.PSR vlOO. LARS 6.10.04
 Triangle Laboratories, Inc.®
 801 Capitola Drive • Durham. North Carolina 27713
 Phone: (919) 544-5729 • Fax: (919) 544-5491
                                 Printed: 14:06 09/18/97
                                       142

-------
Data Review  By:
Initial    ....Date...
          £L/.!!/3:
                     Calculated Noise Area: n/a
The Total Area  for each peak with  an  ion abundance ratio outside
ratio limits  has been recalculated according to method requirements.
Page No.
09/18/97
Listing of  S975833B.dbf
Hatched GC  Peaks  / Ratio / Ret. Time
Compound/
H_Z ---- QC.Log Omit Why  . .RT. OK Ratio Total .Area. .. Area . Peak . 1 ..  Area. Peak. 2. . Rel.RT Compound. Name. .  ID..  Flags.
TCDF
304-306
 304-306









D
D


DC
DC
DC
DC
DC
DC


DC
DC


NL
SN
SN
SN
SN
SN


SN
SN
2

0:
17:
18:
18:
19:
19:
19:
20:
20:
22:

00
36
12
29
09
28
54
23
54
15
0.
RO
RO
RO
RO
RO
RO
RO



65-
1.
0.
0.
0.
0.
1.
1.
0.
0.
0.
0.89
14
58
21
31
44
14
22
70
81
69
Peaks
                                               0.12
                                               2.64
                                               1.08
                                               1.52
                       2.34
                       3.08
                      10.04
                      31.84
                       5.81
                       7.40
                      41.38
                                                            6.90
                                                           13.16
                                                     0.820-1.101
                                                        0.000
                                                        0.364
                                                        0.894
                                                        0.908
                                                        0.940
                                                        0.956
                                                   5.67  0.977
                                                  18.68  1.001  2378-TCDF
                                                        1.026
                                                        1.092
                                                                                                     AN
 13C12-TCDF
 316-318
 316-318

DC
DC






NL 0:
WL 19:
19:
19:
20:
20
20

00
11
:31
:53
:22
:52
:59
0.
RO




RO
RO
65-
1.
0.
0.
0.
0.
0.
1.
0.89
69
73
75
80
77
61
18
5 Peaks

0.
141.
15.
48
6,305
22
6
6,398

87
,93
.12
.40
.72
.14
.92
.30



6.
21,
2,733,
9
4




.48
,58
.69
.63
.63




8.
26
3,572
15
3

O.i


,64
.82
.03
.74
.91

                                                    0.951-1.049
                                                        0.000
                                                        0.942
                                                        0.958
                                                        0.976
                                                        1.000  13C12-2378-TCDF ISO
                                                        1 .025
                                                        1.030
                                      Above: TCDF / TCDD Follows
 TCDD
 320-322
  320-322
0.65-0.89
DC
DC
DC
DC
DC
DC
DC
DC

DC
DC
DC
DC

NL
SN
SN
SN
SN
SN
SN
SN

SN
SN
SN
WH
1
0:
18:
18:
18:
20:
20:
20:
20:
21
21
21
22
22
00
06
13
52
04
23
43
:56
:12
:31
:52
:22
:40
RO

RO
RO
RO
RO
RO

RO
RO
RO
RO
RO
a.
0.
1.
0.
1.
2,
0,
0
0
0
0
0
1
14
81
22
57
,09
,28
.58
.83
.56
.40
.21
.30
.18
Peak
0.
0.
1.
1.
0.
2.
0,
0,
12
0
0
0
1
12
12
67
66
17
41
,16
.60
.42
.60
.39
.78
.41
.38
.60
                                                             5.48
                                                    0.853-1.059
                                                        0.000
                                                        0.854
                                                        0.859
                                                        0.390
                                                        0.947
                                                        0.961
                                                        0.977
                                                        0.987
                                                   9.82  1.000 2378-TCDD
                                                        1.015
                                                        1.031
                                                        1.055
                                                        1.069
                                                                                                      AN
  37C1-TCDD
  328
                 DC  NL
                          0:00
                         19:39
                        0.06
                      130.92
                                                            130.92
                                                      0.906-1.094
                                                          0.000
                                                          0.927
 Triangle Laboratories, Inc.®  Analytical Services Division
 801 Capitola Drive • Durham, North Carolina 27713
 Phone: (919) 544-5729 • Fax: (919) 544-5491
                                                                       Printed: 14:07 Ott1 W

-------
Page No.
09/18/97
Listing of S975833B.dbf
Matched GC Peaks  / Ratio /  Ret. Time
Compound/
M_Z.... QC.Log Omit Why ..RT. OK Ratio Total.Area... Area.Peak.1.. Area.Peak.2..  Rel.RT Compound.Name..  ID.. Flags.
328
13C12-TCDD
332-334





332-334
PeCDF
340-342








21:13
2 Peaks
3,
4,
881.
012.
17 3,881.17
09
0.65-0.89
DC NL 0:
19:
20:
21:
21:
22:
00
52
59
12
34
41
RO




RO
1.
0.
0.
0.
0.
0.
5 Peaks

DC NL 0:
DC SN 22:
DC SN 22:
DC SN 23:
23:
DC SN 24:
DC SN 24:
24:
DC SN 25:

00
34
56
39
49
14
23
43
00
1 .
RO

RO
RO
RO
RO


RO
25:29
DC SN 25:46
DC SN 25:57
DC WH 26:44

340-342
13C12-PeCDF
352-354







352-354
PeCDD
356-358






DC WH 27;
:00
RO
RO
RO
32-
0.
1.
0.
0.
0.
0.
1.
1.
3.
1.
1.
0.
4.
67
79
81 6,
80 4,
78
59
11,
1.78
18
67
72
45
87
82
44
66
05
36
,69
,67
.47
1.29
3 Peaks

DC NL 0
23
24
24
25
25
DC SN 25
26

:00
:48
:20
:42
:00
:28
:45
:28
1.
RO





RO

2.
29.
317.
816.
78.
5.
247.
Tf*nr
i wUL
0.
5.
1.
1.
7.
71
49 13.01
39 2.820.24
30 2,138.52
21 34.15
82 2.53
21

15
48
41
60
57 4.60
0.76
2.90
63.
1,
58
,12 39.40
.50
.09 33.43
1.21
0
0
2
128
.81
.87
.06
.78
32-1.78
0
1
1
1
1
1
2
1
6 Peaks

DC NL 0
DC SN 23
DC SN 24
DC SN 25
DC SN 25
25
DC SN 25

:00
:54
:12
:29
:39
:51
:59
1
RO
RO
RO
RO
RO

RO
.32
0
0
0
5
1
1
0
. 38
.51
.66
.55 5
.55
.59 4
.36
.47
10
-1.78
.86
.06
.23
.78
.96
.67
.46
0
211
28
,398
41
,680
5
16
.12
.92 127.42
.69 17.89
.40 3,280.01
.06 24.96
.89 2,870.11
.92
.36 9.74
1.
001 37C1-TCDD
SUR1
0.906-1.094
0.
16.48 0.
3,497.15 0.
2,677.78 1.
44.06 1.
4.29 1.

0.907-
0.
0.
0.
0.
5.26 0.
0.
0.
23.72 1.
1.
24.66 1.
1.
1.
1.
000
937
990 13C12-1234-TCDD
000 13C12-2378-TCDD
017
070

1.078
000
914
928
957
964
981
987
001 12378-PeCDF
012
032 23478-PeCDF
043
051
082


RSI
I SI











AN

AN



1.093



0.838-1.162
0,
84.50 0,
10.80 0
2,118.39 1
16.10 1
1,810.78 1
1
6.62 1
.000
.964
.985
.000 13C12-PeCDF 123
.012
.031 13C12-P6CDF 234
.043
.072



IS2

SUR2


,377.32
PeCDF / PeCDD Follows —
0
1
2
1
0
38
1
.10
.48
.06
.28
.64
.74 24.22
.00
0.921
0
0
0
0
0
14.52 1
1
-1.026
.000
.925
.936
.986
.992
.000 12378-PeCDD
.005






AN

Triangle Laboratories, Inc.® Analytical Services Division
801 Caprtola Drive • Durham, North Carolina 27713
Phone: (919) 544-5729 • Fax: (919) 544-5491
                                                                  Printed: 14:07 09/18/97
                                                                                 144

-------
Page No.
09/18/97
Listing of  S975833B.dbf
Hatched GC  Peaks / Ratio /  Ret. Tine
Compound/
M_2....  QC.Log Omit Why . .RT. OK Ratio Total .Area. .. Area. Peak. 1. .  Area. Peak. 2. . Rel.RT Confound. Name..  ID..  Fl*««.


356-358
13C12-PeCDD
368-370




368-370
HxCDF
374-376

D










374-376
13C12-HXCDF
384-386










384-386
HxCDD
390-392




DC SN 26:31 RO 0.53
DC WH 26:54 RO 3.33
1 Peak
1.32-1.78
DC NL 0:00 RO 1.00
DC SN 24:42 RO . 2.75
DC SN 24:53 RO 2.05
25:51 1.49
25:59 1.63
2 Peaks
1.05-1.43
DC NL 0:00 1.20
DC SN 27:23 RO 1.48
DC SN 27:30 1.40
DC SN 27:43 RO 5.48
DC SN 27:49 RO 0.46
DC SN 28:00 RO 1. 98
DC SN 28:04 1.35
28:22 1.43
28:29 1.14
DC SN 28:41 1.15
29:00 1.17
DC SN 29:34 RO 6.00
29:42 1.08
4 Peaks
0.43-0.59
DC NL 0:00 0.54
27:21 0.50
27:30 0.50
28:21 0.51
28:28 0.50
DC SN 28:47 RO 0.23
28:59 0.50
29:13 RO 0.74
DC SN 29:29 RO 0.29
29:41 0.49
DC SN 29:53 RO 0.27
7 Peaks
— lV^rtT7
1.05-1.43
DC NL 0:00 1.22
DC SN 28:23 RO 1.67
DC SN 28:29 RO 2.54
DC SN 28:36 RO 0.36
DC SN 28:41 RO 1.76
1.45
0.77
38.74

0.12
5.81
6.30
3,485.93 2,084.63
335.10 207.75
3,821.03
P»f T"in / HvTTlP Fnl 1 nurs — — -
. r&\~ULs I nx\rLfc f OA .L ows — — •
3.25
3.02
6.12
0.60
1.38
2.35
1.62
42.35 24.95
48.34 25.72
1.89
37.58 20.23
0.63
38.79 20.11
167.06

4.98
26.79 8.96
69.75 23.40
3,668.30 1,230.99
4,602.27 1,532.26
1.48
4,273.95 1,421.97
7.90 3.86
2.22
3,176.71 1,044.27
5.60
15,825.67
o • Hvf*rn7 i Uvonn Tr^l 1 nuc
6 ; nxi. Uf i rtxiw uu e o ± i ows
3.13
4.66
3.16
0.96
0.85
1.026
1.041

0.845-1.155
0.000
0.956
0.963
1,401.30 1.000 13C12-PeCDD 123
127.35 1.005

0.955-1.052
0.000
0.962
0.966
0.974
0.977
0.984
0.986
17.40 0.996 123478-HXCDF
22.62 1.001 123678-HxCDF
1.008
17.35 1.019 234678-HxCDF
1.039
18.68 1.043 123789-HxCDF

0.859-1.141
0.000
17.83 0.961
46.35 0.966
2,437.31 0.996 13C12-HXCDF 478
3.070.01 1.000 13C12-HXCDF 678
1.011
2,851.98 1.018 13C12-HXCDF 234
5.23 1.026
1.036
2.132.44 1.043 13C12-HXCDF 789
1 .050

0.950-1.015
0.000
0.972
0.975
0.979
0.982







I S3










AN
AN

AN

AN





SUR3
IS4

ALT 2


ALT1








 Triangle Laboratories, Inc.® Analytical Services Division
 801 Capitals Drive • Durham, North Carolina 27713
 Phone: (919) 544-5729 • Fax: (919) 544-5491
                                                                      Printed 14:07

-------
Page No.     4
09/18/97


Compound/
M_Z.... QC.Log Omit  Why
Listing  of S975833B.dbf
Matched  GC Peaks / Ratio / Ret.  Tin
.RT.  OK Ratio Total.Area... Area.Peak.1.. Area.Peak.2.. Rel.RT Confound.Name..  ID.. Flags.





390-392
13C12-HXCDD
402-404




402-404
HpCDF
408-410




408-410
13C12-HpCDF
413-420


N

413-420
HpCDD
424-426





424-426
13C12-HpCDD
436-438


436-438
DC SN 28:55 RO
DC SN 29:00 RO
29:08
29:13
29:30
3 Peaks
l.<
DC NL 0:00 RO
28:35
29:07
29:12
29:29
4 Peaks
0.
DC NL 0:00 RO
DC WL 31:00 RO
31:12 RO
DC SN 32:06 RO
32:25
2 Peaks
0.
DC NL 0:00 RO
31:11
DC SN 31:29 RO
32:25
DC SN 32:39 RO
2 Peaks
0.
DC NL 0:00 RO
31:26
DC SN 31:45
32:04
DC WH 32:18 RO
DC WH 32:22 RO
2 Peaks
0
DC NL 0:00 RO
31:27
32:04
2 Peaks
3.35
2.13
1.39
1.22
1.23

35-1.43
0.99
1.29
1.23
1.21
1.21
1
88-1.20
2.11
2.71
1.26
3.91
1.03

37-0.51
1.28
0.42
0.78
0.42
0.78

.88-1.20
1.79
1.12
0.91
0.94
3.13
1.84

.88-1.20
0.70
1.00
0.99

0.38
2.15
20.26 11.78
29.32 16.09
32.56 17.95
82.14

4.12
22.18 12.51
2,527.73 1,393.53
3,578.12 1,960.48
4,703.04 2,577.69
.0,831.07
HvOnf^ / UrifTVfi* I?*-il 1 ^Mife
nxt-UJJ / fipCLJr r onows ---
1.55
0.92
37.27 23.11
0.47
20.34 10.56
58.11

1.48
3.165.84 939.83
2.33
1,653.99 489.01
2.82
4,819.83
: HpCDF / HpCDD Follows —
0.80
5.82 3.07
0.90
28.45 13.79
0.31
2.84
34.27

3.02
24.31 12.16
3,368.32 1,672.82
3,392.63
». Ursr-nn / rw-i-a-r^nn smA rm
0.990
0.993
8.48 0.998 123478-HXCDD AN Q
13.23 1.001 123678-HxCDD AN
14.61 1.010 123789-HXCDD AN

0.966-1.034
0.000
9.67 0.979
1,134.20 0.997 13C12-HXCDD 478 SUR4 Q
1,617.64 1.000 13C12-HXCDD 678 IS5
2,125.35 1.010 13C12-HXCDD 789 RS2

0.995-1.044
0.000
0.994
18.27 1.001 1234678-HpCDF AN
1.029
10.28 1.040 1234789-HpCDF AN

0.936-1.128
0.000
2,226.01 1.000 13C12-HpCDF 678 IS6
1.010
1,164.98 1.040 13C12-HpCDF 789 SUR5
1.047

0.976-1.006
0.000
2.75 0.980
0.990
14.66 1.000 1234678-HpCDD AN
1.007
1.009

0.969-1.031
0.000
12.15 0.981
1,695.50 1.000 13C12-HpCDD 678 IS7

 Triangle Laboratories, inc.®  Analytical Services Division
 801 Caprtola Drive • Durham, North Carolina 27713
 Phone: (919) 544-5729 • Fax: (919) 544-5491
                                                                    Printed: 14:07

-------
Page No.
09/18/97
        Listing  of  S975833B.dbf
        Hatched  GC  Peaks  / Ratio / Ret.
                                       Tin
Compound/
M_Z.... QC.Log Omit Why ..RT. OK Ratio Total.Area... Area.Peak.1. .  Area.Peak.2. . Rel.RT Compound.Name.. ID.. Flags.
OCDF
442-444
 442-444
0.76-1.02
DC
DC
DC
DC
DC
DC
DC
DC
DC
DC
DC
DC
DC
DC
DC

DC
DC
DC

NL
SN
SN
SN
SN
SN
SN
SN
SN
SN
SN
SN
SN
SN
SN

SN
SN
SN
1
0:
30:
31:
31:
32:
32:
32:
33:
33:
33:
33:
33:
34:
34:
34:
34:
35
35
35
00
55
32
51
13
35
55
04
21
38
46
59
08
18
:24
:44
:26
:34
:56
RO
RO
RO
RO
RO
RO .
RO
RO
RO
RO
RO
RO
RO
RO
RO

RO
RO
RO
0.
0.
2.
1.
7.
0.
1.
1,
1
0,
2
0
0
1
0
0
1
0
1
12
43
15
73
00
,67
.15
.18
.34
.58
.96
.22
.46
.61
.56
.88
.91
.47
.20
Peak
0.
1.
0.
1.
0.
1.
1.
1.
1.
1.
1.
0.
0.
0.
0.
27.
1,
1,
3
27
13
08
49
25
11
53
51
49
17
85
02
23
87
53
96
,70
.55
.55
.29
.70
                                                            0.884-1.116
                                                                0.000
                                                                0.893
                                                                0.911
                                                                0.920
                                                                0.931
                                                                0.941
                                                                 .951
                                                                 .955
                                                             13.00
                                                                          14.70
                    0.
                    0.
                    0.963
                    0.972
                    0.975
                    0.982
                    0.986
                    0.991
                    0.994
                    1.003  OCDF
                    1.024
                    1.027
                    1.038
 OCDD
 458-460
 458-460
               0.76-1.02
DC  ML   0:00     0.86
        34:38     0.94
      1 Peak
                                                0.13
                                               55.85
                                               55.85
27.09
                0.884-1.116
                    0.000
             28.76  1.000 OCDD
 13C12-OCDD                    0.76-1.02
 470-472         DC  NL   0:00 RO  2.34          0.72
                         34:37     0.86      4,277.10
                 DC  WH  34:59 RO  1.61          3.21
 470-472               1  Peak                4,277.10
                                         1,971.86
                 0.995-1.005
                     0.000
           2,305.24   1.000 13C12-OCDD
                     1.011
                                                                                       IS8
 Column Description.
                "Why" Code Description	  QC Log Desc.
 M_Z   -Nominal Ion Mass(es)
  ..RT. -Retention Time (mm:ss)
 Rat.l -Ratio of M/M+2 Ions
 OK    -RO=Ratio Outside Limits
 Rel.RT-Relative Retention Time
      End of Report
                WL-Below Retention Time Window  A-Peak Added
                WH-Above Retention Time Window
                SN-Below Signal to Noise Level
                
-------
rile:5975833 #1-048 Aogill-S£P-1997 12:18:52 21+ Voltage SIX
70S Mbid«i39
303.9016 F:2 BSU*(2S6, 30, -3. 0) PXD(9,5,5, 0.05\,156 .0,1.00\,F,T) XxptETCOS
TRIANGLE LABS T*Xt:0-H23-FB TLH43085 1X7. TIME - 12:21
1001
80J
60:
40:
20:

Al


A6.90X4
i
Jll "Ff A1.99E4 111
... i. ^ JL..A.. -A-,. ,ju 	 M,. JL. K.iA.l\lt *
17:00 18:00 19:00 20:00
225


\
A2.fOX4
\ |L A3. 02X4

.2.9X4
.2.4X4
.1.824
.1.224
.5.9JE3

21(00 22s 00 XisA
rile !S9 75833 #1-840 Acg:ll-SrP-1997 12:18:52 EH- Voltage SIX 70S Noi*»:33
305.8987 F:2 BSUB(256, 30, -3.0) ta>(9,5,S,0.05\rL32.0r1.00\,F,T) Exp:EPCUS
TRIANGLE LABS T«xt:O-K23-FB TLH43085
1001
80:
60.
40:
20:
0'
Al


AS. 67X4
A1.99X4 A1.21E4 lf[
17:00 18:00 19:00 20:00
UOr. TIKE - 12<21
7*5 -4.1X4

\

\
\ rk/\ A9.82E3 ~fj^\ 1
.J.224
.2.424
.1 . 524
.8.123
O.OEO
21:00' 22:00' Tijie
File:S975833 #1-848 Acq:ll-SEP-1997 12:18:52 EI+ Voltage SIR 70S Noiae:415
315.9419 F:2 BSUB(256,30,-3 .0) PKD(9,5,5, 0. 05\,1660. 0,1 . 00%,
TRIANGLE LABS Taxt:O-M23-FB TLI#43085
1003
80:
60:
40:
20:
o:
A2





171-00 18:00 	 191-00 ' '20:00
r, T) Exp : EPCUS
IIU. TIME - 12:21
• 73JT7 6.5E6




1 {
_5.225
Lj . 925
.2.525
.1.326
O.OEO
'21:00 ' 22.- 00 ' ' Mj»e
rile:S975833 #1-848 Acq:ll-SEP-1997 12:18:52 EI+ Voltage SIR 70S Jfci»e:247
317.9389 r:2 BSOB(256, 30, -3 . 0) PKD(9, 5,5, 0 .05\,988.0, 1.00\,F,T) Exp:EPCUS
TRIANGLE LABS Text:O-M23-FB 111*43085
lOOi
80J
60.
40.
20.
0.
A3





17:00 18:00 19:00 20:00
IttJ. TIME ' 12:21
JE7 8.6X6





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21\00 ' ' ' '22.- 00 ' Tine
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|l7:10i7.a0 I / AL 1. 19:1* 15»45i j
• ULAJU_M_OAAJ^JL/ A*uuJO_A_A-_AAAAAA^*M_JjuA_»JL L
17:00 18:00 19:00 ' 20:00

IKJ. TIME ' 12 i 21
C1.5X4

21:53
i

» 20,45 21.37 »f«
i.Jftfcj\AAA\A LA^^A^ AA/^/l VX^^L^^uA^
.1.2X4
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f a. oxo
21:00 22:00 Tijie
148

-------
FlletS975833 #1-848 Aoqill-SXP-1997 12:18:52 EI+ Voltage SIM 708
319.8965 Fi2 BSV*(256,30,-3.0) rKD(7,5,3,0.05\,1144.0,1.00\rr,T)
TRIANGLX LABS Text:O-M23-FB TLH43085 XX7.
1001 AS. 4
80J
001 A2.78X4
40J A 1
1 jl I A3. 53X3 I
4 ll « na u \ 1 1 1 1
"1 rl~ /^flA -J^JU .. .. A A AiAv/^/lAj*/»M/W\A^wv^»A\-AwwAAvJVwVAA'>'V\™-_A/V/' u.n.ii«Ax JUMJT i
	 19:00 20:00 21:00
Noi*et286 1
XxptXrCUS
TIM* - 12:21
8X4
\ -
\ A5.04X3
1
1 A5.51« 1 1 -
\*i.69*3 flln , i *J. i, ft -
I^»A !.«.. /LJurUUK/MIU^/JiL Iku
V^AftAHArtyv*/**!!*! WL/»IV lui^ABf»iV»A^'''"-j •
1.5X4
1.0X4
7.7*3
5.1*3

2.6X3
0.0X0
22 i 00 Time
Jile :SS 75833 91-848 Acqill-SXP-1997 12:18:52 XJ+ Vbltag* SIM 70S Noifet35
321.8936 Fs2 BSVB(256,30,-3.0) PKD(7,5,3,0.05\,140.0,1.00\,F,T)
TRIANGLX LABS Text:O-M23-FB TLH43085 IKT.
1001
80:
60l
40:
20:

A9.



Al . 11X4 1
A 8 . 4 6X3 i Ag U£l
.*w ..... AA. A A .A.-». _ . -AJ~, 	 w^^uAjta-.KAA^AA — JlA~V/
15:00 20:00 21:00
XxpiKPCUS
TIME - 12s 21
82X4



\ Al . 60X4
V^Aj*. AAj'VA..A^r>jAJlVAA^'W
2.5X4
2.0X4
.1.5X4
.9.5XJ
.5.0*3
0.0X0
22:00 Time
File:S975833 #1-848 Acq:ll-SEP-1997 12:18:52 EI+ Voltage SIR 70S Noiae:1280
331.9368 F:2 BSDB(256, 30, -3. 0) PKD(7, 5, 3,0 .051,5120.0,1. 00\,F,T) ExpsEPCUS
TRIANGLE LABS Text:0-M23-FB TLH4308S INJ
100J
80J
soj
40:
20.

A2 B2E7
A2.



l U
19:00 20:00 21:00
TIME - 12:21

14X7
\
\


V
.5.9X5
.5.5X6
.4.1X6
•.2.7E6
_1 . 4X5
0.0X0
22:00 Time
File:S975833 #1-848 Acqill-SEP-1997 12:18:52 EI+ Voltage SIR 70S Noiae:767
333.9338 F:2 BSOS(256, 30, -3 .0) PKD(7,5, 3, 0. 05\, 3068. 0,1 . 00\,F,T) Eip-.EPCUS
TRIANGLE LABS Text:O-M23-FB TLI#4308S IJTJ. TIME - 12:21
1003
80:
60:
40:
201

AJ.sor?
U2.6flr7



/ \>
19:00 20:00 21:00



V
.8.5X5
16.5X5
1.5.2X5
1J.4X5
.1 . 7X6
0 . 0X0
22:00 Time
File:S975833 fl-848 Acqsll-SEP-1997 12:18:52 EI+ Voltage SIR 70S Noiae:31
327.8847 F:2 BSOB( 256, 30, -3 . 0) PKD(7, 5, 3, 0. 051,124 . 0,1. 00%, F, T) Exp:EPCUS
TRIANGLE LABS Text:O-M23-FB TLI#43085 IWJ". TIME ' 12:21
1001
80.
60.
40.
20.
0
A3





19:00 20:00 21:00
{E7





1 . 0X7
L8.1X6
:6.1X6
.4.0X6
.2.0X6
O.OEO
22:00 Time
File:S975833 fl-848 Acq:ll-SEP-1997 12:18:52 EI+ Voltage SIR 70S
330.9792 Fs2 ExpiEPCUS

TRIANGLE LABS TexttO-M23-FB TLI*43085 I«J. TIHX - 12:21
100
80
60
40
20
0
t 18-51 19*31 I54?2w?i^S 21-0




':
2 /^4^^v£5ios 22:20 -^





-5.7X6
r •
.4.6E6
'.3.4E6
.2.3X6
.1.1X6
0.0X0
	 15:00 20:00 21:00 22:00 Tim*
14

-------
rile: 3975833 #1-848 Aoqtll-SXT-1997 12:18:52 XI+ Voltage SIM 70S Hoia»:43
339.8597 n2 BSU*(256, 30, -3.0) PKS(7,5,3
TMIANGLE LABS Text:0-M23-TB TLI#43085
1003

80:
50:
40.
20.
:
o:






A3.43E4 A4.60X4
23:00 2ife:253
341.8567 Ts2 BSUB(256, 30, -3.0) PKD(7,5.3, 0 .05\r 1012.0,1 .00\,F. T) XzptXPCUS
TRIANGLE LABS TextiO-H23-FB TLI#43085
1003
80:
50:
40.
20:
o:




A5.26E4
IHJ. TIME - 12:21
A2.37X5 A2.47X5 7.5X4
I
n n

.. .J
A1.19E4 M A1.11E4 1 \ AJ--f*8 I A1.03X4 A1.12X4.
•^s***~* ~~**Y***-As*i\m AJJMTVW f~*1~. 	 1 1^— / — w: — ?TV^A Xi1 "rt — A A1 r. — R — / — \~r~n — m*.n 	 '~nrz — rr — V; IT n — • ' -"' •• — n 	 n 	 • — *-r* •.- .A.
.6.0X4
.4.5X4
.3 . 0X4
.1 . 5E4

23*00 24:00 25iflO 2Sl-00 ' ' ' life
Tile:S975833 #1-848 Acq:ll-SEP-1997 12:18:52 EH- Voltage SIX 70S KOiae:36
351.9000 Ti2 BSUB(256,30,-3.0) PKD( 7, 5, 3, 0. 05\,144.0,1. 00\,T, T) XxptEPCUS
TRIANGLE LABS Text:O-M23-FB TLH43085
100}
.
so:
50:
40!
20:
0:






^^^^^
TWT. TIME - 12:21
A3. 28X7 ,.1.1X7
k A2.87X7
ft A
ft


/ V /I

.8.6X6
.6.4X6
.4.3X6
.2.1X6
• n nrn
23:00 24\00 25:00 25:00 	 Time
File:S97S833 #1-848 Acq:ll-SEP-1997 12:18:52 XI+ Voltage SIX 70S KOiae:39
353.8970 T:2 SSUB(256,30, -3 .0) PKD(7,5,3, 0. 054,155. 0,1. 00%, T, T) Exp:EPCUS
TXIANGLE LABS Text:O-M23-FB TLI#43085
1003
80:
50:
40:
20:
o:






INJ. TIME - 12:21
A2.





•2E7 6.9X6
Al . 81X7
1



V 1 i.
.5.5rff
.4. 1X6
.2.7X6
ll . 4X6

23:00 24:00 25:00 26:00 	 Time
Tile:S975833 #1-848 Acq:ll-SEP-1997 12:18:52 Eli- Voltage SIX 70S
330.9792 F:2 ExptEPCOS
TRIANGLE LABS Text : O -M2 3 -TB TLI#43085
1001

80:
50J
40J
20J
OJ
23 • 12 23 * 32 24 t 0
_r^v.j^^^vN^^^^^-^^-A\x^vV-'
-tyvr/g"^^^^
•wV^^




JWJ. TIME - 12:21
i 24:19 24*49 25*23 ST'^l o*c IT *• .——
s-s*rv**s**f---*--^r-*~*t ~-~\ x-^w^vs. /V-^^A. />^i^ *£?J^ 26:35
v V^ >/ ^^^**%x v^*s "^^*^"^wv»
^-^^^




.0.11.0
.5 . 1X6
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.2.6X6
.1 . 3X6

23:00 24:00 25:00 26\00 ' ' ' Time
rile:S975833 #1-848 Acqtll-SEP-1997 12:18:52 EI+ Voltage SIX 70S
409.7974 F:2 ExptXPCOS
TRIANGLE LABS Text:O-M23-n TLI#43085
100]
80J
50J
.
401
201
ol
1NJ. TIME - 12:21
1 24:05 C8.8X3
II
22.-U2
1 ill 22s 53
11 1
fill 1 ft. 1 23:40



26, 3
Aii^A/
.7.0X3
.5.3X3

.3.5X3
.1 . 8X3
33l°° 24:00 25:00 ' 26\00 	 M»c
150

-------
Tll*iSy/5»33 tl-»4U Acq:ll-SEF-1997 11118:52 XI* Voltage SIX 70S Nolf*:JJ
355.8546 T:2 BSUB(256,30, -3 .0) PKD(7 ,5,3,0 .05\, 128. 0,1. 00\,T,T) XxptXPCUS
TXIANGLX LABS Text:O-M23-n TLIt4308S IXT. TXHX - 12:21
10M
SO.
50.
40.
20.


A2.42X5
1
^
'

,. .
A1.25X4 A1,35C4 A7.50X3 A1.02X4 * '* * 1 \ AI'f5rf '

24:00 ' 25<00 26*00
0.2X4
6.514
t.»X4
3.3*4
1.6X4

9.0*0
Time
r±l»:S975833 #1-048 Acqi ll-SEP-1997 12:18:52 XI+ Voltage SIX 70S Holme : 37
357.8516 t:2 BSUB(256, 30, -3.0) PKV( 7,5, 3,0. 05\,148 .0,1.00\,r, T) XxpiXPCUS
TRIANGLE LABS TfJCt:0-K23-FB TLH43085 IVJ. TIME - 12:21
1003
80.
•
60:
40.
20.
OJ
A1.46E5
A A1.45Z5


I A5.43E4
1 \ l\
1 L,JVrA7".J\^ ^JWJ^^jSS _J
/\


tjbKr_";r..
24:00 25:00 26:00
.4.9X4
.3.8*4

.2.9X4
.1.9E4
.9 . 6X3
O.OEO
Time
r±le:S975833 #1-848 Acij:ll-SEP-1997 12:18:52 EI+ Voltage SIR 70S Koine -.36
367.8949 1:2 BSUB( 256, 30, -3 . 0) PXD(7, 5,3,0. 05\, 144 .0, 1.00\,F,T) Exp:EPCUS
TRIANGLE LABS Text:O-M23-FB TLH43085 IHJ. TIKE - 12:21
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rlle:S975833 #1-848 Acq: ll-SEP-1997 12:18:52 EH- Voltage SIR 70S Ko±ae:35
369.8919 T:2 BSUB(256,30, -3.0) PKD(7,5, 3, 0.05\,140. 0,1. 00\,T, T) Exp:EPCUS
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rile:S975833 #1-848 Acq: ll-SEP-1997 12:18:52 EI+ Voltage SIR 70S
330.9792 F:2 ElptEPCUS
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TSIANGLX LABS Text:O-M23-FB TLI#43085
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375.8178 F:3 BSUB(256,30e -3.0) PXD(7,5,3,0
TRIANGLE LABS Text:O-M23-FB TLI#43085
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ril«:S975833 #1-405 Acsr.-ll-SW-.Z9P7 12:18:
383.8639 F:3 BSUB(256,30, -3 . 0) PJO>(7,5,3,0
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TRIANGLE LABS Text:O-M23-FB TLI#43085
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File:S975833 #1-406 Acq:ll-SEP-1997 12:18:52 EI+ Voltage SIS 70S
392.9760 F:3 Exp:EPCUS
TS I ANGLE LABS Text:O-M23-FB TLI#4308S
1003
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File:S975833 #1-406 Acq:ll-SEP-1997 12:18:52 Eli- Voltage SIS 70S
445.7555 F:3 Xxp:XPCVS
TRIANGLE LABS Text:O-M23-FB TLI#43085
1003
80:
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401
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|
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152

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riJ.*lSy/5BJ3 #1-406 AOJlJ.l-SKf-1997 12iL9>52 XI+ VoJtag* SI*  70S Hoi»»taSB
389.8156 ri3 BSUB(256, 30, -3.0)  PXD(7, 5,3, 0 .051,3432.0,1. 00\,r,T) XxpttPCOS
TXIAHSLK LASS  T*XtlO-M23-fB TLII43085                     J1K7. TIM* -  12(21
1001                                                                      AI.79X5
  80.

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     27(40   20(00   20(12    20(24   28:36   20(40    29(00
rile:3975833 41-406 Act}:ll-SEP-1997 12(10(52 XX+ Voltage  31X1703 Naif*:704
391.8127 T:3 BSUB(256,30,-3.0) PKD(7,5,3,0.051,2816.0,1.00\,r,T) ExpiEPCUS
TRIANGLE LABS  TtattO-M23-FB  TLH43Q85                      INJ. TIME -   12(21
1001                                                         JU.32X5     A1.46E5
  80.
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                                                                                2936   294»
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\ril»,S975633 tl-430 Aoqtll-SXP-1997 13:18,52  11+ Volt*?* SIX 70S Moif0,802
 407.7818 Ts4 B9OB(256,30,-3.0) PXD(7, 5,3,0.05\,3308.0,1.00\,T,T) XzpiXTCUS
 TRIANGLE LABS  T9fttO-H33-FB  TLH43085                      OKT. TlttX "   13t21
 1001

  80:

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  40.

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           A3.31X5
                                                                        Al.06X5
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            31:12     31:24      31,36     3l't48      32', 00      32,13     32,24      32:36
 rileiS975S33 tl-430 Acqill-SXP-1997 13,18,52 XI* Voltage SIX 70S Nolle,382
 409.7789 r,4 BSUB(256,30,-3.0)  PXB(7,5,3r0.05\,1538.0,1.00\,r,T) XxptXPCOS
 TXIASGLX LABS  TexttO-H33-FB 11.1*43085                     JKT. TIMX -  13t31
                                                                                             32,48
                                                                                                       .0.0X0
                                                                                                          Time
 1001
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  60:
  40:
  20:
               3X5
                                                                        Al.03X5
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                                                   A4.30X3
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 rile,S975833  tl-430 Aojsll-SEP-1997 13,18:53 EH- Voltage  SIR  70S Stoife,658
 417.8253 T:4  BSUB(256,30,-3.0) PKD(7,5,3,0.05\,2632.0,1.00\,r,T)  ExpiEPCOS
 TRIANGLE LABS  Tejct:O-M23-FB  TLIt4308S                     JKT.  TIME -   12,21
          A9.40X6
                                                                        A4.89E6
                                                                                               32,48
                                                                                                       O.OEO
                                                                                                          Tim,
   80:
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             31,12     31,24     31,36      31,48     32:00      32:12     32,24     32,36
  rile,S975S33 #1-430 Acq,ll-SEP-1997 13,18:53  EH-  Voltage SIR 70S Boiae:513
  419.8220 F:4 BSUB(256,30,-3.0) PKD(7,5,3,0.05\,2052.0,1.00\,F,T) Exp:EPCUS
  TRIANGLE LABS  Text,O-M23-TB  TLH43085                      ISJ. TIKE -   12,21
  1004     A2.23E7

   80:

   60:

   40:

   20:

    oj	
                                                                                                32:48
                                                                                                        O.OEO
                                                                                                           Tim
             31,12     31:24      31:36     31,48      32,00      32:12
  Tile,S975833 tl-430 Acq:ll-SEP-1997 12,18,52 EI+ Voltage SIX 70S
  430.9729 r,4 Eip-.EPCUS
  TRIANGLE LABS  Tsjct,O-H23-rB   TLI#430BS                     Z1KT. TIMS -
                                               31,51      ,„.„„      32,14
                                                                        A1.16E7
 .5.4X6

 .4.1X6

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                                                                           32,24
                                                                                      32:36
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                                                                                                         Tim
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                                                        ^32:02
                                                                           12:21
                                                                                32:32
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             31,12      31,34     31:36      31,48      33,00     32:12      32:34
  rile,S975833 tl-430 Acq:ll-SEP-1997 13:18:53 Eli- Voltage SIR  70S
  479.7165 T:4 EipiEPCUS
  TRIANGLE LABS  Text:0-M33-fB  TLH43085                     JW7.  TIME -   13,31
  1001
                                                                                    33:36
                                                                                              33:48
  .0. OEO
     Tim
             31:13
                        31:34
                                  31,36
                                             31,48
                                                       33,00
                                                                 32:12
                                                                            33:34
                                                                                      33:36
                                                                                                 33,48
                                                                                                          154'

-------
F1J.»:SS758JJ H-4JO Aoqtll-SEP-lS97 12:18:52 XI+ VOltMye SIX 70S HO1M»:348
423.7766 T:4 BSUB(256, 30, -3 .0 ) PKD( 7,5, 3,0 .05\, 1392.0,1 .00\,r,T) IxptXTCUS
TRIANGLE LABS T*xt:O-M23-FB TLH4308S IK7. TIMS - 12t21
1001
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File:S975833 #1-430 Acqtll-SXP-1997 12:18,52 XH- Voltage SIR 70S Noise: 197
425.7737 T>4 BSUB(256, 30, -3.0) PKD(7, 5,3, 0 .05\, 788.0, 1.00\,F,T) ExpiXPCOS
TRIANGLE LABS TeitiO-H23-TB TLH43085 IK7. TIME - 12i21
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Time
rile:S975833 11-430 Acq: ll-SEP-1997 12:18:52 EI+ Voltage SIR 70S Noiae:770
435.8169 T:4 BSOB(256, 30, -3 .0) PKD( 7,5,3, 0. 05\,3080. 0,1 . 00\,F, I) Exp:EPCDS
TRIANGLE LABS Teit:O-H23-FB TLI«430B5 TK7. TIME - 12:21
100J
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0
A1.67E7
A
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L8.7E5
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Time
r±le:S975833 «1-430 Acq: ll-SEP-1997 12:18:52 EI+ Voltage SIR 70S Ko±ae:1101
437.8140 T:4 BSUB(256, 30, -3. 0) PKD( 7,5,3, 0.05\,4404. 0,1. 00%, f,T) Exp:EPCUS
TRIANGLE LABS TextiO-M23-FB TLI#43085 I1KT. TIME - 12:21
1001
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Time
Tiles S975833 fl-430 Acq: ll-SEP-1997 12:18:52 EI+ Voltage SIR 70S
430.9729 T:4 EzpsEPCUS
TRIANGLE LABS Text:O-H23-FB TLI (43085 ISJ. TIME - 12:21
100
80
60
40
20
0
^ 31:22 31s29 31:36 31:42 3{t** 3a.oa J^v5~- fV*J\ y^^
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-------
   *,sy/3ejj fi-«ju AcqtJ.i-ssf-j.ay/ utioisa EI+  vojicag* si* /us noim»,jy
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  IANGLX LABS  T*XttO-M23-r*  TLXH3085                      XX7. TIM* -    12131
 001                                 A3.;
 80.
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 40.
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  04-
      34t24         34130         34:36         34,42         34,46         34,54
 iletS975833 H-430 Acqill-SEP-1997 12,18,52 11+ Volt*ye SIS  70S  ttoimms33
 59.7348 T,4 BSOB(256,30,-3.0)  PKD(7,5,3,0.05\,132.0,1.00\,T,T) SxptEPCOS
TRIANGLE LABS  T«Xt:O-M3J-fB TLH430S5                     INJ.  TIME -   12,21
 001
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      34:24         34:30         34:36         34:42         34:48         34:54
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 69.7779 r,4  BSUB(256r30,-3.0) PU>(7,5,3,0.05\,1784.0,1.00\,T,T) ExpiEPCOS
TRIANGLE LABS  T»lt:O-H23-rB  TLH43085                      IKT. TIME -   12:21
1001                                A1.97E7
       34,24         34,30         34:36        34:42        34:48         34:54
rile:S97S833 #1-430 Aoqtll-SEP-1997 12:18:52  EH- Voltage SIS 70S JK>iae:192
471.7750 T:4 BSOB(256,30,-3.0) PKD(7,5,3, 0.05%,768.0,1.00\,r,T) Eip:EPCUS
TRIANGLE LABS  Text:0-M23-FB  TLH43085                      UKT. TIME »   12:21
100*
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       34:24         34:30         34:36         34:42         34:48
 F±le:S975833 #1-430 Acqsll-SEP-1997 12:18:52 EI+ Voltage SIX  70S
 430.9729 r:4 ExpiEPCUS
 TRIANGLE LABS  T*rt:0-H23-FB  TLH43085                     INJ.  TIME -
34:54
                                                                             12:21
 1003

  80.

  60.

  40.

  20.

   0.
                                                                       34:52
             35,00
             35:00
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                                                                                                 -2.2E6

                                                                                                 '.1. 8E6

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       34:24
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                     .4.6X5
                     34,30
                                   34s 36
                                                 34142
                                                               34:48
                                                                             34,54
                      .0.0X0
              J5JOO       Time

-------
Channel    I  338,3792     Peak top
Height  3,25 udts  Span  288 pp«

Systei file na*EPOJS2
Data   fdenaie         fl=$911971
Resolution                  18868
Group matter                    2
lonlzklon aode              El*
Switching                 VOLTflGE
Ref, masses   232,3825,   416.3788
ft   293      J  331      3   368
B   384      K  332      T   378
             L  334      U   376
             H  348      V   418
             N  342
             0  352
             P  354
             9  356
             R  358

 Ref,  lass   416.3768    Peak top
 Height    ,72 volts  Span   288 ppi
15

-------
'ile:S975833 #1-848 Acq:ll-SfiP-1997 12:18:52 EI+ Voltage SIR 70s
19.8965  F:2 Exp:EPCUS
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-------
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.00%                          31A11                                                      .-2.9E6
80J                           A                                                        L2.3E6

60-                           I  \                                                        L1.7E6
40J                           /  \                                                       L1.2E6

20J                          /   \                                                      L5.8E5
 i — I — i — i
30:48
i — i — I — i — i
 31:00
                             31:12
                                     i — i — i — | — i — i — i — i — i — I — i — i — i — i — i — | — i — i — i — i — i — I — i — i — i — i — i — | — i — i — r-
                                       31:24     31:36     31:48     32:00     32:12
O.OEO
   Time

-------
>ile:S975833 '11-430 Acq:ll-SfeP-19'97  12:18:52  EI+  Voltage SIR 70S
141.7428 F:4 Exp:EPCUS
.'ample Text :O-M23-FB  TLI#43085                      INJ.  TIME =    1.2,:21  File Text :O-M23-FB  TLI>
L00%                                                            f^Al. OE5)
        31:00           32:00           33:00           34:00
'ile:S975833 #1-430 Acq:ll-SEP-1997 12:18:52 EI+ Voltage SIR 70S
:43.7399 F:4 Exp:EPCUS
lample Text :O-M23-FB  TLI#43085                     INJ. TIME =   J^L:21_J?ile Text:O-M23
                                                                   O.OEO
                                                                      Time
                                                                  FB  TLI»
                                                                   2.2E4
                                                35:00
        31:00           32:00           33lOO           34:00
'ile:S975833 #1-430 Acq:ll-SEP-1997 12:18:52 EI+ Voltage SIR 70S
69. 7779  F:4 Exp:EPCUS
iample Text:O-M23-FB  TLI#43085                     INJ. TIME =   12:21 File Text:O-M23
.00%                                                             34;37

80 j

60J

40 j

20J
       31:00
1   I	1	1-
32:00
-i	1	1	1	r
 33:00
                                                      -i	1	1	r
                                                      34:00
                                                                                         .O.OEO
                                                                                            Time
                                                                                        FB  TLI»
                                                                                         2.2E6

                                                                                        L1.8E6

                                                                                        L1.3E6

                                                                                        _8.9E5

                                                                                         4.4E5
35:00
O.OEO
   Time

-------
TLI Project:      43085
Client Sample:   O-M23-FB
                                         Method 23 TCDD/TCDF Analysis (DB-225)
                                                              Analysis File:   P973861
Client Project:
Sample Matrix:
TLI ID:

Sample Size:
Dry Weight:
GC Column:
S413-004
M23Train
181-55-4ABD

1.000
n/a
DB-225

Date Received:
Date Extracted:
Date Analyzed:
Dilution Factor:
Blank File:
Analyst:

09/03/97
09/04/97
09/13/97
n/a
P973852
JM

Spike File:
ICal:
ConCal:
% Moisture:
% Lipid:
% Solids:

SPC2NF04
PF22206
P973859
n/a
n/a
n/a
Analytes
Amt. (ng) PL
f-MPC Ratio
8T
Flags
2,3,7,8-TCDF
                              ND
0.05
 Internal Standard
                                                                  Ratio
"C,2-2,3,7,8-TCDF
                              2.8
                                             70.9
           40%- 130%
                                                                   0.77     20:38
 Recovery Standard
                                                                  Ratio
                                  RT
13C12-1,2,3,4-TCDD
                                                                   0.82
                                                                            19:40
                      Data Reviewer
                                      O/l     / ,
                                     - ^r _?_ * ' r^-' i - '>
                                          Page 1 of 1
                                                               09/18/97
Triangle Laboratories, Inc.®
801 Capitola Drive • Durham, North Carolina 27713
Phone: (919) 544-5729 • Fax: (919) 544-5491
                                                                         Printed: 15:53 09/1

-------
                       Initial
                                  	Date...
Data Review By:
          J~    ^ / (*£/  I-T Calculated Noise Area:    1.26
The Total Area for each peak with an ion abundance ratio outside
ratio limits has been recalculated according to method requirements.
Page No.
09/13/97
         Listing  of P973861B.dbf
         Matched  GC Peaks  / Ratio / Ret. Time
Compound/
M_Z.... QC.Log Omit Why ..RT.  OK Ratio Total.Area... Area.Peak.1.. Area.Peak.2.. Rel.RT Compound.Name..  ID.. Flags.
TCDF
304-306

304-306
               0.6S-O.S9
DC  NL   0:00     0.81
DC  SN  20:39 RO  0.46
      0 Peaks
                                              2.01
                                              1.17
                                              0.00
                               0.786-1.095
                                   0.000
                                   1.001 2378-TCDF
                                                         AH
 13C12-TCDF
 316-318
                DC
                DC
               0.65-0.89
         0:00 RO  0.96
                  2.63
                   NL
                   WL  19:21  RO
                       19:38  RO  2.07
                        20:38
                                  0.77
 316-318
                 DC  WH  22:11 RO  3.45
                      2 Peaks
  2.64
  1.29
  2.96
249.60
  0.55
252.56
                                                              3.45
                                                            108.39
    0.952-1.048
        0.000
        0.938
  1.67  0.952
141.21  1.000  13C12-2378-TCDF ISO
        1.075
                                       Above: TCDF / TCDD Follows
 13C12-TCDD                     0.65-0.89
 332-334         DC  NL   0:00  RO  2.30          1.43
                         19:26      0.79        204.62
                         19:40      0.82        253.67
                 DC  SN  20:19  RO  0.93          2.41
 332-334               2 Peaks                 458.29
                                             90.32
                                            114.52
                                                                            0.897-1.103
                                                                                0.000
                                                                        114.30  1.000 13C12-2378-TCDD IS1
                                                                        139.15  1.012 13C12-1234-TCDD RSI
                                                                                1.045
 Column Description	  "Why" Code Description	  QC Log Desc.
 M_Z   -Nominal Ion Mass(es)
  . .RT. -Retention Time  (mm:ss)
 Rat.l -Ratio of M/M+2  Ions
 OK   -RO=Ratio Outside Limits
                                                 A-Peak Added
                                                 K-Peak Kept
                                                 D-Peak Deleted
                               WL-Below Retention Time Window
                               WH-Above Retention Time Window
                               SN-Below Signal to Noise Level
                               
-------
Voltmg* 3IS 7 OP
'11*,P973B61 tl-755 Aoy,13-SxP-1997  11,57,55
03.9016 SjcptDB225
 TANGLE LABS  Tmxt:O-M33-n  TLIt43085
  21:00    21:12     21:24     21:36    21:48     22:00    22:12
r±le:P973861 fl-755 Atxj:13-SEP-1997 11:57:55 EH- Voltagre SIS 70P
319.8965 ExpsDB225
TRIANGLE LABS  Text:0-M23-FB TLH43085
100$                      21:30
                                                                     22:24
                                                                               22:36
                                                                                                    f O.OEO
                                                                                        22:48
                                                 21:58
                                                       22:06
                                                                         22:29
                                                                                  22:40       22:55
                                                                                         22:49
  45:

  40.

  35.

  30l

  25.

  20.

  15J

  10.
                                                                                                  23:00  Time
                                                     8.5E3

                                                     8.1E3

                                                     7.6E3

                                                     7.2X3

                                                     6.8E3

                                                     6.4E3

                                                     .5.9E3

                                                     .5. 5E3

                                                     .5.1E3

                                                     .4.7E3

                                                     .4.2E3

                                                     -.3. 8E3

                                                     .3. 4E3

                                                     .3.0E3

                                                     .2.5E3

                                                     .2.1S3

                                                     :1. 7X3

                                                     .1.3X3

                                                     .8.5X2

                                                     .4.2X2
  31  00
            31113
                      21:24
                                21:36
                                         31:48
                                                   22100
                                                            22113
                                                                      32134
                                                                               23136
                                                                                         22:48
                                                 r^_-.0.0X0
                                                  23 00  T±M
                                                                                                         164

-------
 •1J.»:P973B6± tl-733 AoqtJ.J-SXP-1997 Ui57l55 EI+ Volt*g»  SIM70P Hoim»l450
 03.9016 BS03(25«,30r-3.0) PKD(5,3,1,0.10\,1800.0,0.00\,r,r)  Xzp:DB225
TXIANGLE LABS  T»*t.tO-K23-TB TLIt43085
 00\
            17100         IB'tOO         19,00         20100         21:00
 ile:P973861 tl-755 Aoq:13-SXP-1997 11>57>55  EI+ Voltage SIS 7OP No±fm,554
 05.8987 BSOB(2S6,30,-3.0)  PKD(5,3,1,0.10\,3216.0,0.00\,T,r) Xxp:DB225
TXIAHGLX LABS  T»JCt:O-M23-rB TLH4308S
 00\                                                         A1.12K4
22tOO
             17:00        IS', 00         19': 00         20:00        21iOO
 F±le:P973B61 tl-755 Acqtl3-SEP-1997 ll:S7i55 EH- Voltaga  SIX  70P HO±aet714
  15.9419 BSUB(25S,30,-3.0)  PKD(5,3,1,0.10\,2856.0,0.00\,F,r)  SxptDB225
 TRIANGLE LABS  TexttO-H23-TB TLH430B5
 1001                                                        A1.Q8E6
  80.

  60.

  40:

  201
22iOO
             17:00         10:00        25:00         20:00         21:00
 rileiP973861 tl-755 Acqil3-SEP-1997 11:57:55  EI+ Voltage SIX 70P Hoiaet747
 317.9389 BSOB(356r30,-3.0) PKD(5,3,1,0.10\,2988.0, 0.QO\,T,T) ExpsDB225
 TRIANGLE LABS  T&Xt:O-M23-FB  TLHH3035
                                                                                  22:00
 1003

  801

  SO.

  40.

  301
                                                              A1.41E6
             17 \ 00         18,00         19:00         20,00        21:00
 rlleiP973861  tl-755 Ac?>13-SEP-1997 11:57:55 11+ Voltuga  SIX  70P
 375.8364 Exp:DB225
 TRIANGLE LABS  T*xt:O-M33-rB TLH43085
 1003k
 22:00
              17,00
                            18:00
                                         19:00
                                                       20100
                                                                     21100
                                                                                   22100
                 3. OE5

                 .2.4X5

                 .1. 8E5

                 .1.2X5

                 .6.1X4
                 .0.0X0
                     T±m
                 3. 8X5

                 ,3.1X5

                 .2.3X5

                 .1. 5X5

                 .7.7X4
                 .0.0X0
                     T±m
                                                     19t54                21:22
                                                            20:21 20:44
                                                                                                      165.

-------
                   ISiOO             19!00             SOiOO              31.00
Flle,P973861 #1-755 Aoq:13-SXP-1997  Ili57i55 XI+ Voltage SIX 70P Halfft518
 31.8936 BSUB(256r30,-3.0) PXD(5,3,1, 0.10\,2073.0fO.OO\,F,F) Kxp:DB225
TRIANGLE LABS  Text:O-K23-FB  TLH43085
10(71
 80.
'Ile:py73861 91-755 AoqiJ.J-SKP-J.SS7 ll:S7lSS XI + Voltage SIM  70P HOim»:SlJ
 19.8965 B3UB(256,30,-3.0) PKD(5,3,1,0.10\,3048.0, 0.00\,r,r)  Xxp:DB325
 tlAHSLX LABS  TexttO-M33-FB TLH43085
 00\
               AS.12X3
                                    A6.55X3
                                                       ^4.4X3
                                    A4.40X3
                                                                                               .88X31
                                               32,00
                                                            T±mt
                   18,00              19:00              20:00              21:00
r±le:P973B61 #1-755 Acq:l3-SEP-1997 11:57:55 SI+ Voltage SIX TOP M&iae.-515
327.8847 BSUB(256,30,-3.0)  PKD(5,3,1,0.10\,2064.0, 0.00\,r,T) ExptDB235
  JAWCir LABS  Text>O-M23-rB TLH43085
1003,                                         A1.S2E6
  so:

  so:

  40:

  30.
                    18:00             19:00             20:00             31:00
 Til*:P973861  #1-755 Acg:13-SEP-1997 11:57:55 EI+ Voltage SIX  70P Mai«et928
 331.9368 BSUB(2S6,30,-3.0) PKD(5,3,1,0.10\,3712.0,0.00\,r,r)  Exp:DB225
 TRIANGLE LABS  Tfat:O-M23-FB TLIt43085
 1001                                            A1.J.5E6
  80J

  601

  401

  20L
   o:
A9.03E5
                   18*00              ISsOO              20:00              21:00
F±le:P973861 #1-755 Acq:13-SXP-1997 11:57:55 XI+ Voltage SIS 70P Hoiae:403
333.9338 BSOB(356,30,-3.0)  PKD(5,3,l,0.10\,1612.0,0.00\rF,F)  Xlp:DB225
TRIANGLE LABS  Text:O-M33-FB TLI*43085
                                                 A1.39X6
                                            A1.14E6
 80J

 60.

 40.

 30.

  0.
                    18:00
                                               22: 00
                                                22:00
                                                                                             22:00
                                                        .4.3ES

                                                        '.3.4X5

                                                        -2.6X5

                                                        .1. 7X5

                                                        .8.6X4
                                                                                                     0.0X0
                                                                                                        Tim
                                                                                                    -3.1X5

                                                                                                     .2.5X5

                                                                                                     .1. 9X5

                                                                                                     .1.3X5

                                                                                                     .6.3X4
                                                                                                      .0.0X0
                                                                                                         Tim
                                       19:00
                                                         20100
                                                                           31:00
                                                                                             22:00
                                                         .3.8X5

                                                         .3.0X5

                                                         .2.3X5

                                                         '.1.5X5

                                                         .7.6X4

                                                          0.0X0
                                                             Xlm)
                                                                                                       166

-------
ni*i
303. i
TXXJU
1004
^
40:
sol
0.
Tile
315..
TXIAi
100J
80J
50J
40:
sol
File
319.
XRIA
1001
Bol
60l
401
SO.
0.
rile
331.
TRIA
1001
aol
6ol
401
aol
o-
r±ie
293.
TXIt
1003
80.
60.
40.
20.
0.
rilt
330
TXI1
100!
80.
60.
40.
20.
0
P973861 41-755 Aoqil3-SXT-1997 Ili57i55 XI + Voltage SIM 70P
1016 Exp:DB225
KLX IMS TmxttO-H23-FB TLH43085
H^^^
17(00 18(00 19(00 20(06 21<00 ' 22(00
IP973861 #1-755 Acq,13-3i:P-1997 11(57(55 II* Voltage SIX 70P
9419 EiptD3225
ttSLE LABS TtxtiO-M23-FB TLH43085
20t38
1
17(06 18(00 19(00 20(00 21(00 22(06
(P973851 *l-755 Acqtl3-SEP-1997 11(57(55 EH- Volt»ge SIX 70P
8965 Exp -.03225
NC£JT LABS T*xt:O-M23-TB TLI»43085
I 17(50 20 t 19 21 (JO
17(06 18(00 IPl'OO 20(00 21(00 22(06
IP973861 #1-755 Acqtl3-SEP-1997 11(57(55 JEI+ Voltage SIX 70P
9368 EipsDB225
NSLE LABS TeJCt:O-M23-FB TLH43085
19 -.40
"il
III
17(06 18.'o6 15(06 20(00 21(00 22(00
(P973851 #1-755 Acq:13-SEP-1997 11:57:55 EI+ Voltage SIS 70P
9825 ExptDB225
\XSLE LABS Text:0-M23-fB TLI*43085
1.^^15^55^17(21 17(54 18:20 18(5019(15 19(4tf 20(47 21(47 22(45

17(06 ' 18:00 ' ' 19(00 20(00 ' 21(06 22(06
»(P9738ffl #1-755 Ac9:13-srP-1997 11(57(55 EH- Voltage SIX 70P
9792 ExptDB225
UIGLS LABS TextiO-M23-rB TLI4430B5
^J£«2917(0<> i7. 53 18(47 19(49 20.-J9 21:24 22-01 32,42
• T^^f^ I " *— V*w>V-''V-~vw ^v*~ w»^**> -~" •'» f\j^jr~***s*-. T>^^Asr^-i^yV- ,«,,.,^.. . .. .^..-^^.-.^^--u.v
j V
.a. 4X3
.7.5K3
.5.7X3
.3.9X3
.1.9X3
0.0X0
Am
.3.1X5
.2.5X5
.1 . 8X5
.1.2X5
.6.2X4
0 . 0X0
Time
.9.4X3
-7.5E3
.5.7X3
.3 . 8X3
.1 . 9X3
.0.0X0
Time
3.2E5
.2. 6X5
.1.9X5
.1.3E5
.6.4X4
• Q OEO
rue
-9.5E5
:7.7E6
.5.8X6
.3 . 8X6
.1.9X6
.0.0X0
Time
..1.217
9.6X6
7.3X6
4.8ft
.2.4X6
•o.oxo
17(00 18(06 19(06 20(00 21(06 ' ' ' 22(06 ' Tim*

-------
fef.  tass    292,9825    Peak top
Height   1.61 volts  Span  288 ppi
Systa file naie
]ka   file naie
Resolution
Group ruter
lonlzatlon Mde
Switching
Ref, lasses   292.9825,
  fi:P973861
    292.9825
    383.9816
    385.8987
    315.9419
    317.9389
    319.8965
    321,8936
    327,8847
    338,9792
J
K
L
I
       1
     El*
 VQLTRGE
388.9761
338.9792
331.9368
333,9338
3^,8364
 Channel   I  336.9792    Peak top
 Height  1,83 volts  Span  266 pet
                                                                           168

-------
TLI Project:      43085
Client Sample:   I-M23-1
Method 23 PCDD/PCDF Analysis (a)
             Analysis File:  S975834
Client Project:
Sample Matrix:
TLI ID:

Sample Size:
Dry Weight:
GC Column:
S413-004
M23Train
181-55-5ABD

1.000
n/a
DB-5
Date Received:
Date Extracted:
Date Analyzed:
Dilution Factor:
Blank File:
Analyst:
09/03/97
09/04/97
09/11/97
n/a
S975815
BJG
Spike File:
ICal:
ConCal:
% Moisture:
% Lipid:
% Solids:
SPX23704
SF56117
S975814
n/a
n/a
n/a
: • ; ••••;•;--.--_•: ; 	 ;. r :.• -f ;.;.; .
Analytes .--• •••••;?:v:-': •
2,3,7,8-TCDD
1,2,3,7,8-PeCDD
1,2,3,4.7,8-HxCDD
1,2,3,6,7,8-HxCDD
1,2,3,7,8,9-HxCDD
1,2,3,4,6,7.8-HpCDD
1,2,3,4,6,7,8,9-OCDD
2,3,7,8-TCDF
1,2,3,7.8-PeCDF
2,3,4,7,8-PeCDF
1,2,3,4.7,8-HxCDF
1,2,3,6,7,8-HxCDF
2,3,4,6,7,8-HxCDF
1,2,3,7,8,9-HxCDF
1,2,3,4,6,7,8-HpCDF
1,2,3,4,7,8,9-HpCDF
1,2,3,4,6,7,8,9-OCDF

$0W*;* ;,,.,> ;^=v:
Total TCDD
Total PeCDD
Total HxCDD
Total HpCDD
Total TCDF
Total PeCDF
Total HxCDF
Total HpCDF

-;•• :::-;v.r::-^int^ (ng)
ND
ND
ND
ND
ND
ND
9.7
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND

^.4;f.l:.:VAnBt(tng)
ND
ND
ND
EMPC
EMPC
0.47
ND
ND

01. EMPC?-
0.06
0.2
0.2
0.2
0.2
0.3

0.05
0.09
0.09
0.1
0.1
0.1
0.2
0.2
0.2
0.3

Number DL EMPC
0.06
0.2
0.2
0.35
0.18
1
0.1
0.2
j^ * .Afe^fe •"* ^mm
R«tK> 8T t^fcgs






0.93 34:43








	


- .-\ ^ flags



—



_.
                                        Pagel of 2
                           X237.PSR rlOO. LARS 6.1904
  Triangle Laboratories, Inc.®
  801 Caprtola Drive • Durham, North Carolina 27713
  Phone: (919) 544-5729 • Fax: (919) 544-5491
                        Printed: 14:07

-------
    Project:      43085
 iient Sample:   I-M23-1
       Method 23 PCDD/PCDF Analysis (a)
                    Analysis File:   S975834
Internal Standards
3C,2-2,3,7,8-TCDF
!Ci:-2,3,7,8-TCDD
'CiZ-l,2,3,7,8-PeCDF
3C,2-l,2,3,7,8-PeCDD
3Cp-l,2,3,6,7,8-HxCDF
'C,:-l,2,3,6,7,8-HxCDD
'Cr.-UJA^S-HpCDF
3C,:-l,2,3,4,6,7,8-HpCDD
3Cp-l,2,3,4,6,7,8,9-OCDD

Surrogate Standards {Type A)
7CL-2,3,7,8-TCDD
3C,2-2,3,4,7,8-PeCDF
3Ci2-l,2,3,4,7,8-HxCDF
3C,;-l,2,3,4,7,8-HxCDD
3Cr-l,2,3,4,7,8,9-HpCDF

Alternate Standards (Type A)
JC,2-l,2,3,7,8,9-HxCDF
3C,2-2,3,4,6,7,8-HxCDF
Recovery Standards i : iy;
3C!2-1,2,3,4-TCDD
3CI2-l,2,3,7,8,9-HxCDD
Ami (ng)
2.9
2.9
2.0
1.8
26
2.8
2.2
2.4
4.5

Arift. (ng)
4.1
3.7
47
3.6
44

Arat: (ng) ;;:
3.2
3.1
'•:•; i.;: ;;--: • ="•• ;' /K..


%R»covwy
72.8
73.3
50.6
45.4
654
70.9
56.0
59.6
558

^;;'^1R*coverr
102
92.1
117
89.9


f^v.%;^coyery
80.6
76.4
V;" ..;.|::.::.;.;'::d|;;|'.- . ;>.,.


QC Limits
40%-130%
40%- 130%
40%-130%
40%- 130%
40%- 130%
40%- 130%
25%- 130%
25%- 130%
25%- 130%

: OgUmits
70%- 140%
70%- 140%
70%- 140%
70%- 140%
70%- 140%

; : QG: Limits
40%-130%
40%- 130%



Ratio
0.74
0.87
1.56
1.56
051
1.24
0.43
1.04
0.79

Ratio

1.49
054
1.22
045

Ratio
0.51
0.52
Ratio
0.86
1.17
, wr
21:09
21:51
25:08
26:12
28-42
29:23
31:21
32:10
34-45

RT
21:52
25:52
28-36
29:18
32-31

8T"i'f
29:53
29:12
HT
21:37
29:40
Fiags



Q_
n
Q_
Q_
Q 	
O

Flags


Q
Q_
o
V 	
•;:Ftegs;k
Q_
Q 	
FNjs^I

Q 	
                     Data Reviewer
't -K-L<-i-'O
                                        Page 2 of 2
09/18/97
                                  X237.PSR V2.00. LARS 6.10.04
Triangle Laboratories, Inc.®
301 Capitola Drive • Durham, North Carolina 27713
3hone: (919) 544-5729 • Fax: (919) 544-5491
                               Printed: 14:07 09/18/97
                                         170

-------
                       Initial
                                   . .Date. .
Data Review By:
                     Calculated Noise Area:
                                                                      1.48
The Total  Area for each peak with an ion  abundance ratio outside
ratio limits has been recalculated according  to method requirements.
Page No.
09/18/97
Listing of S975834B.dbf
Matched GC Peaks  /  Ratio / Ret. Time
Compound/
M_Z.... QC.Log Omit Why  ..RT. OK .Ratio Total.Area... Area.Peak.1..  Area.Peak.2..  Rel.RT Compound.Name.. ID.. FLmg*.
TCDF
304-306
 304-306
 13C12-TCDF
 316-318
 316-318
 TCDD
 320-322
  320-322
0.65-0.89
DC
DC
DC
DC
DC

DC


DC
DC
DC

DC


DC
DC
DC
DC
DC
DC
DC
DC
DC
DC
DC
DC
DC
DC
DC
DC
NL
SN
SN
SN
SN

SN
1

NL
WL
SN

WH
1

NL
WL
SN
SN
SN
SN
SN
SN
SN
SN
SN
SN
SN
SN
SN
SN
0:
18:
18:
18:
19:
19:
20:
00
16
35
55
17
35
03
RO
RO
RO
RO

RO
RO
0.
0.
0.
1.
0.
0.
0.
29
97
59
30
68
95
52
Peak

0:
19:
20:
21:
22:

00
54
43
09
17
0.
RO
RO
RO

RO
65-0.89
1.
0.
0.
0.
3.
14
32
31
74
12
Peak

0:
18
18
19
19
19
19
20
21
21
21
21
21
22
22

:00
:09
:53
:08
:47
:55
:59
:33
:OS
:21
:33
:45
:50
:30
:42
0.
RO
RO

RO
RO
RO
RO
RO
RO
RO
RO

RO
RO
RO
22:46 RO
65-0.89
1
0
0
0
3
0
0
1
2
1
8
0
0
4
1
1
.00
.64
.69
.40
.33
.94
. 94
.36
.00
.04
.17
.73
.43
.86
.74
.67
0 Peaks
                                               0.46
                                               2.76
                                              13.49
                                               1.43
                                               6.72
                                              14.07
                                               7.40
                                              14.07
                                               0.12
                                               0.76
                                               1.40
                                             257.05
                                               1.19
                                             257.05
                                                    0.820-1.101
                                                        0.000
                                                        0.864
                                                         .879
                                                         .894
                                                         .912
                                    7.55
                                                  7.95
                                                          926
                                                        0.948
                                   109.18
                                      Above: TCDF / TCDD Follows
                                               0.12
                                               0.53
                                               1.00
                                               1.29
                                               0.42
                                               0.35
                                               0.30
                                               0.99
                                               1.13
                                               0.44
                                               0.
                                                 .11
                                                 ,02
                                                 .24
                                                0.50
                                                 .20
                                                 .13
    0.951-1.049
        0.000
        0.941
        0.980
147.87  1.000 13C12-2378-TCDF  ISO
        1.054
                                                      .853-1.059
                                                        0.000
                                                        0.831
                                                        0.864
                                                        0.876
                                                        0.905
                                                        0.912
                                                        0.915
                                                        0.941
                                                        0.965
                                                        0.977
                                                        0.986
                                                        0.995
                                                        0.999  2378-TCDD
                                                        1.030
                                                        1.039
                                                        1.042
                                                                                                      AN
                                                0.00
  37C1-TCDD
  328
                 DC  NL   0:00
                 DC  WL  18:06
                 DC  WL  18:09
                 DC  WL  18:28
                        0.06
                        1.64
                        0.50
                        1.24
     0.906-1.094
         0.000
         0.828
         0.831
         0.845
 Triangle Laboratories, Inc.®  Analytical Services Division
 801 Capitola Drive • Durham, North Carolina 27713
 Phone: (919) 544-5729 • Fax: (919) 544-5491
                                                                       Printed; 14:08 08/1&97
                                                                                                               111

-------
 Page No.

 09/18/97
Listing of S975834B.db£

Matched oc PeaXs /  Ratio / Ret. Tin
 Compound/

 M_Z....  QC.Log Omit Why ..RT.  OK Ratio Total.Area..
                                                  Area.Peak.1.. Area.Peak.2.. Rel.RT Compound.Name..  ID.. Flags.
DC
DC
DC
DC
DC
DC
DC
DC
DC
DC
DC
DC
DC
DC
DC
DC
DC
DC
DC
DC
DC
DC
DC
DC
328
13C12-TCDD
332-334 DC
DC
DC
DC
DC
DC


DC
DC
DC
332-334
PeCDF
340-342 DC
DC
DC

DC
WL
WL
WL
WL
WL
WL
WL
WL
WL
WL
WL
SN
SN
SN
SN
SN
SN
SN
SN
SN
SN
SN
SN
SN
3
NL
WL
WL
WL
WL
SN


SN
SN
SN
3
NL
WL
WL

SN
18:35
18:42
18:46
18:59
19:03
19:14
19:20
19:23
19:26
19:38
19:45
19:59
20:10
20:24
20:31
20:42
20:59
21:09
21:15
21:20
21:27
21:38
21:52
22:13
22:23
22:30
22:37
Peaks
0
18
18
19
19
21
21
21
22
22
22
22
Pe
0
22
22
23
24
:00
:36
:58
:09
:42
:20
.37
:51
:08
:23
:33
:37
aks
:00
:26
:45
:12
:19
0.
RO
RO
RO
RO
RO


RO
RO
RO
RO
1.
RO
RO
RO


65-0.89
38.33
0
3
12
17
0
0
0
1
1
0
2
32
1
0
0
1
1
.31
.03
.56
.00
.68
.86
.87
.76
.99
.91
.95
-1.78
.17
.62
.90
.52
.66
0.
0.
0.
0.
0.
0.
0.
0.
0.
0.
0.
0.
5.
0.
0.
0.
0.
0.
0.
0.
0.
0.
180.
9.
0.
1.
0.
195.
0.
1.
1.
0.
0.
2.
268.
209.
6.
1.
1.
25
40
09
45
59
,50
,38
16
38
SO
22
77
65 5.65
32
15
70
35
55
53
26
94
55
26 180.26
74 9.74
95
38
22
65
.11
,06
,19
,57
30
89
06 124.01
.33 97.44
02 5.97
,24
,65
0.97
483.41
TCDD / PeCDF Follows 	
0.12
0,
1
20
7
.63
.02
.10 12.11
.23
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
1
1
1
1
1
0.906
0
0
0
0
0
0
144.05 0
111.89 1
3.40 1
1
1
1
0.907
0
0
0
7.99 0
0
.850
.856
.859
.869
.872
.880
.885
.887
.889
.899
.904
.915
.923
.934
.939
.947
.960
.968
.973
.976
.982
.990
.001 37C1-TCDD SUR1
.017
.024
.030
. 035
-1.094
.000
.851
.368
.376
.902
.976
.989 13C12-1234-TCDD RSI
.000 13C12-2378-TCDD IS1
.013
.024
.032
.035
-1.078
.000
. 882
.894
.912
.956
Triangle Laboratories, Inc.® Analytical Services Division
801 Capitola Drive • Durham, North Carolina 27713
Phone: (919) 544-5729 • Fax: (919) 544-5491
                                                                 Printed: 14:0809/18/97
                                                                                 172

-------
Page No.
09/13/9-7
Listing  oC S975834B.db«
Hatched  GC Peaks / Ratio  / Ret. Time
Conpound/
M_Z....  QC.Log Omit Why ..RT. OK Ratio Total.Area...  Area.Peak.1. .  Area.Peak.2. .  Rel.RT Compound.Name. .  ID..  Flag*.
340-342
13C12-PeCDF
352-354







N
N
N



352-354
PeCDD
356-358




356-358
13C12-PeCDD
368-370






N
N
368-370
HxCDF
374-376

DC
DC
DC
DC
DC
DC

DC
DC
DC
DC
DC
DC
DC
DC

DC

DC
DC
DC


DC
DC
DC
DC
DC


DC
DC
DC
DC
DC
DC
DC




DC
DC
SN :
SN ;
SN
SN
SN
SN
1

ML
SN
SN
SN
SN
SN
SN
SN

SN

SN
SN
SN
2

NL
ML
SN
SN
SN
0

NL
SN
SN
SN
SN
SN
SN




NL
WL
24:29
24:39 RO
24:51 RO
25:05 RO
26:36 RO
26:54 RO
Peak
1.3
0:00 RO
22:37 RO
22:43 RO
23:24 RO
23:34
24:03 RO
24:08 RO
24:20 RO
25:08
25:26 RO
25:52
26:20 RO
26:30
26:38 RO
Peaks
1.
0:00 RO
24:04 RO
25:57 RO
26:12 RO
26:33 RO
Peaks
1 .
0:00 RO
24:19 RO
24:26 RO
24:49 RO
25:10 RO
25:31
25:48 RO
26:12
26:20
> Peaks
1
0:00 RO
27:48 RO
1.42
1.14
1.18
0.95
0.34
0.10
12-1.78
1.00
0.46
0.84
1.17
1.37
0.46
0.54
0.99
1.56
2.21
1.49
3.21
1.55
0.77

32-1.78
1.00
9.18
0.62
3.43
0.20

32-1.78
1.00
4.42
0.82
3.28
4.29
1.72
3.93
1.56
1.66

.05-1.43
0.99
1.77
2.18
1.65
3.08
1.04
0.95
0.56
20.10

0.13
0.87
0.89
1.37
0.83
0.41
0.41
2.16
153.70 93.72
1.35
137.24 82.16
O.'M
1.94
2.14
290.94

0.10
0.28
0.53
0.94
0.33
0.00

0.10
0.31
0.77
0.46
0.97
0.68
0.36
77.33 47.13
10.17 6.34
87.50

1.88
3.96
0.963
0.969
0.977
0.986
1.046
1.058
0.838-1.162
0.000
0.389
0.893
0.920
0.927
0.946
0.949
0.957
59.98 0.988 13C12-PeCDF 123 IS2
1.000
55.08 1.017 13C12-PeCDF 234 SUR2
1.035
1.042
1.047

0.921-1.026
0.000
0.914
0.985
0.995
1.008

0.845-1.155
0.000
0.923
0.928
0.942
0.956
0.969
0.980
30.20 0.995 13C12-PeCDD 123 IS3
3.83 1.000

0.955-1.052
0.000
0.952
  Triangle Laboratories, Inc.® Analytical Services Division
  801 Caprtola Drive • Durham, North Carolina 27713
  Phone: (919) 544-5729 • Fax: (919) 544-5491
                                                                     Printed: 14:06

-------
Page No.      4
09/18/97

Compound/
M_Z.... QC.Log Omit Why
                         Listing of S975834B.dbf
                         Matched GC Peaks  / Ratio / Ret. Time
                        .-OT.  OK Ratio Total.Area...  Area.P«ak.l..  Area.Peak.2.. Rel.RT Compound.Name..  ID..  Flags.

















374-376
13C12-HXCDF
384-386









N
N

N




N

384-386
HxCDD
390-392






DC
DC
DC
DC
DC
DC
DC
DC
DC
DC
DC
DC
DC
DC
DC
DC
DC


DC
DC
DC
DC
DC
DC
DC
DC
DC
DC


DC

DC
DC
DC
DC

DC


DC
DC
DC
DC
DC
DC
DC
SN
SN
SN
SN
SN
SN
SN
SN
SN
SN
SN
SN
SN
SN
SN
SN
SN
0

NL
SN
SN
SN
SN
SN
SN
SN
SN
SN


SN

SN
SN
SN
SN

SN
4

NL
WL
SN
SN
SN
SN
SN
27:
28:
28:
28:
28:
28:
28:
28:
29:
29:
29:
29:
29:
29:
29:
30:
30:
:56
14
;35
40
;43
:48
:52
:57
:01
:13
:20
:20
:30
36
42
:06
13
RO

RO
RO
RO

RO

RO
RO

RO
RO
RO
RO
RO
RO
0
1
2
0
6
1
0
1
1
2
1
0
0
1
0
1
4
.67
.37
.90
.90
.08
.10
.74
.34
.02
.74
.19
.98
.14
.01
.93
.95
.89
Peaks

0:
27:
27:
27:
27:
27:
28:
28:
28;

00
28
34
46
49
54
04
07
:13
28t21
28:
28:
28:
29:
29:
29:
29:
29:
29:
30:
:36
42
;53
:12
:20
:25
:33
:38
.53
14
0.
RO
RO
RO
RO
RO
RO
RO
RO

RO


RO

RO
RO
RO
RO

RO
43
0
4
0
2
2
0
0
0
0
1
0
0
0
0
0
1
7
0
0
0
Peaks

0
28
28
28
28
28
29:

:00
:06
:29
:43
:48
•50
:01
1.


RO
RO

RO
RO
05
1
1
5
0
1
1
0
-0.59
.40
.06
.14
.70
.54
.15
.75
.34
.58
.94
.54
.51
.60
.52
.40
.06
.40
.66
.51
.76

-- Above:
-1.43
.41
.14
.10
.11
.07
.02
.53
0.
3.
0.
1.
0,
0,
0.
0.
1.
1.
1.
0.
0.
3.
0.
2.
0.
0.

1.
0.
0.
0.
0.
0.
1.
0.
1.
0,
100.
89.
1
96,
0.
0.
0.
1.
88.
1
374
65
08
47
.26
.54
,88
.63
,89
.99
95
,53
74
78
09
90
89
63
00

66
27
30
.41
.20
.53
09
,47
.15
,72
.38
,20
.34
.55
.92
.71
.23
.28
.59
.37
.72
HxCDF /
1
0
0
0
0
0
1
.47
.60
.22
.16
.85
.81
.19
                                                                               0.957
                                                                               0.967
                                                                               0.979
                                                                               0.982
                                                                               0.983
                                                                               0.986
                                                                               0.989
                                                                               0.991
                                                                               0.994
                                                                               1.001 123678-HXCDF
                                                                               1.005
                                                                               1.005
                                                                               1.010
                                                                               1.014
                                                                               1.017 234678-HxCDF
                                                                               1.031
                                                                               1.035
                                                                                                      AN
                                                                                                      AN
                                                                           0.859-1.141
                                                                               0.000
                                                                               0.941
                                                                               0.944
                                                                                .951
                                                                                .953
                                                                                .955
                                                                                .961
                                                                                .963
                                                                                .966
                                                           35.23
                                                           30.12

                                                           33.07
                                                           29.97
                                                   HXCDD Follows
                                                                                0.
                                                                                0.
                                                                                0.
                                                                                0.
                                                                                0.
                                                                                o.
                                                                                0.971
                                                                          65.15  0.979 13C12-HXCDF 478 SOR3 Q
                                                                          59.08  0.983 13C12-HxCDF 678 IS4  Q
                                                                                0.989
                                                                          63.48  1.000 13C12-HXCDF 234 ALT2 Q
                                                                                1.005
                                                                                1.007
                                                                                1.012
                                                                                •1.015
                                                                          58.62  1.023 13C12-HXCDF 789 ALT1 Q
                                                                                1.035
                                                                           0.950-1.015
                                                                               0.000
                                                                               0.947
                                                                               0.960
                                                                               0.968
                                                                               0.971
                                                                               0.972
                                                                               0.978
Triangle Laboratories, Inc.® Analytical Services Division
801 CapKola Drive • Durham, North Carolina 27713
Phone: (919) 544-5729 • Fax: (919) 544-5491
                                                                                             Printed: 14:08 09/

-------
Page No.
09/18/97
Listing of S975834B.db£
Matched GC Peaks / Ratio  / Rat. Time
Compound/
M_Z....  QC.Log Omit Why ..RT.  OK Ratio Total.Area... Area.Peak.1.. Area.Peak.2.. Rel. RT Compound.Name.. ID.. Flags.
 390-392

 13C12-HXCDD
 402-404
 402-404
 HpCDF
 408-410
 408-410

 13C12-HpCDF
 418-420
         N
         N
         N
 418-420
  HpCDD
  424-426
  424-426

  13C12-HpCDD
  436-438
DC
DC
DC
DC
DC
DC
DC
DC


DC
DC
DC
DC
DC
DC
DC
DC
DC



DC
DC


DC


DC

DC

DC
DC


DC
DC



DC
SN 29:08 1.38
SN 29:14 RO 2.97
SN 29:24 RO 0.37
SN 29:29 RO 0.75
SN 29:34 RO 0.08
SN 29:44 RO 0.25
SN 29:50 RO . 0.77
SN 29:54 RO 0.14
0 Peaks
1.05-1.43
NL 0:00 RO 0.93
WL 27:50 RO 2.14
WL 27:58 RO 1.65
WL 28:19 RO 0.56
WL 28:21 1.35
WL 28:29 RO 0.33
SN 29:00 1.20
SN 29:00 RO 1.48
SN 29:09 RO 0.61
29:18 1.22
29:23 1.24
29:40 1.17
SN 29:50 RO 0.95
SN 29:55 RO 2.02
3 Peaks
0.88-1.20
NL 0:00 RO 1.71
0 Peaks
0.37-0.51
NL 0:00 RO 0.99
31:21 0.43
SN 31:34 RO 0.98
32:31 0.45
SN 32:41 0.49
SN 32:51 RO 0.23
2 Peaks
0.88-1.20
NL 0:00 RO 1.66
SN 31:26 RO 0.39
31:36 RO 0.86
1 Peak
0.88-1.20
NL 0:00 RO 9.63
1.14
0.67
0.56
1.32
0.27
0.31
0.96
0.23
0.00

1.14
0.47
1.46
0.83
1.29
0.34
0.44
0.65
1.45
69.92 38.42
79.95 44.32
113.35 61.18
1.63
1.01
263.22
Uvf T\r\ 1 Ur-vPm? Fril ~\ I-M^C

4.22
0.00

2.02
56.35 17.02
1.50
47.69 14.86
2.00
2.65
104.04

1.63
0.57
5.10 2.60
5.10

0.16
0.982
0.985
0.991
0.994
0.997 123478-HxCDD
1.002 123678-HxCDD
1.006
1.008

0.966-1.034
0.000
0.938
0.943
0.954
0.956
0.960
0.978
0.978
0.983
31.50 0.988 13C12-HXCDD 478
35.63 0.990 13C12-HXCDD 678
52.17 1.000 13C12-HXCDD 789
1.006
1 .008

0.995-1.044
0.000

0.936-1.128
0.000
39.33 0.993 13C12-HpCDF 678
1.000
32.83 1.030 13C12-HpCDF 789
1.035
1.041

0.976-1.006
0.000
0.977
3.01 0.982

0.969-1.031
0.000
W
AN













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 Triangle Laboratories, Inc.®  Analytical Services Division
 801 Caprtola Drive • Durham, North Carolina 27713
 Phone: (919) 544-5729 • Fax: (919) 544-5491
                                                                     Printed: 14:08
                                                                                175

-------
Page No.
09/18/97
Listing of S97S834B.db£
Hatched GC Peaks / Ratio / Ret.  Time
Compound/
M_Z....  QC.Log Omit Why ..RT. OK Ratio Total.Area...  Area.Peak.1..  Area.Peak.2..  Rel.RT Compound.Name..  ID..  Flags.
436*438
                DC  SN  31:35     1.10
                DC  SN  31:40 RO  0.42
                DC  SN  31:59 RO  2.49
                       32:10     1.04
                     1 Peak
                       1.70
                       0.35
                       0.88
                      55.10
                      55.10
28.13
       0.982
       0.984
       0.994
26.97  1.000 13C12-HpCDD 678 IS7
OCDF
442-444
 442-444
	 . 	 ^uj,
0.76-1.02
DC
DC
DC
DC
DC
DC
DC
DC
DC
DC
DC
DC
DC
DC

NL
SN
SN
SN
SN
SN
SN
SN
SN
SN
SN
SN
SN
SN
0
0:
30:
31;
31:
32:
32:
32:
32:
33:
33
33
34
35
35
00
56
30
40
04
:16
:30
:52
:10
:35
:56
:16
:29
:59

RO
RO
RO
RO


RO
RO
RO
RO

RO
RO
1.
0.
1.
2.
0,
0,
0
0
2
2
0
0
0
0
00
,47
.11
.86
.13
.85
.80
.08
.32
.96
.52
.86
.45
.58
Peaks
                                     Above: HpCDD / Octa-CDD and CDF Follows
                       0.12
                       0.70
                       0.34
                       0.42
                       0.32
                       1.33
                       1.76
                       0.38
                       1.89
                       0.43
                       1.91
                       1.06
                       1.68
                       1.70
                       0.00
                  .884-1.116
                     0.000
                     0.890
                     0.906
                     0.911
                     0.923
                      .929
                      .935
                      .946
                      . 954
                     0.966
                     0.976
                     0. 986
                     1.021
                     1.035
 OCDD                           0.76-1.02
 458-460         DC  NL   0:00 RO  1.17          0.11
                        34:43     0.93         38.40
 453-460               1 Peak                   88.40

 13C12-OCDD                     0.76-1.02
 470-472         DC  NL   0:00 RO  0.09          0.11
                DC  WL  34:33 RO  2.02          0.93
                        34:45     0.79         65.71
 470-472               1 Peak                   65.71
                                    42.55
                                     28.91
                                                     0.384-1.116
                                                         0.000
                                                  45.85  0.999 OCDD            AN
                 0.995-1.005
                     0.000
                     0.994
               36.80  1.000  13C12-OCDD      138  Q
 Column Description	  "Why" Code Description	   QC  Log  Desc.
 M_Z   -Nominal  Ion Mass(es)
 ..RT.  -Retention Time  (mm:ss)
 Rat.l  -Ratio of M/M+2  Ions
 OK    -RO=Ratio Outside Limits
 Rel.RT-Relative Retention Time
     End of Report  ***
        WL-Below Retention Time Window
        WH-Above Retention Time Window
        SN-Below Signal to Noise Level
        
-------
Tilei3975834 tl-848 Acqtll-SEP-1997 12:58:11 XI+ Voltage SIX 70S Hoifmi35
319.8965 ri2 BSOB(256,30, -3.0)  PKD(7, 5,3, 0.05\, 140.0,1.00\,r,T) IxptXPCUS
TRIANGLE LABS  TextsI-M23-1   TLI#43085                      IKT. TIMX -   13:00
1001
                                                                                                  .8.0X3
                      ^*"^B&_«^n.^_f^_^&dk_«^i^_U^^_^B^.^^|^UM<^^_^M«L^^«*A^MBK«fli^^^^H^^^i^^Hp_A^4_«&d_
                    19:00              20:00               21:00               22:00
rlle:S975834  tl-848 Acqtll-SEP-1997 12:58:11 EI+ Voltage SIX 70S Hoime:35
321.8936 rt2  BSUB(256,30,-3.0) PXD(7,5,3, 0. 05\,140.0,1.00\,T,T) XxptXPCDS
TRIANGLE LABS  T*xt:I-M23-l  TLIf43085                       IKT. TIME -   13:00

IOU\                                                                            A1.44X4
  80:
  60:
  40:
                  A7.97X3
                                                            AS.62X3

                    19:00               20:00              21:00               22:00
 rile:S975834 tl-848 Acqsll-SEP-1997  12:58:11  EI+ Voltage SIX 70S NoiaesllSO
 331.9368 T:2 BSOB(256,30, -3. 0) PXD(7,5,3, 0. 05\,4600.0,1. 00\,F,T) Exp:EPCUS
 TRIANGLE LABS  Text:I-M23-l  TLIt430S5                      IKT. TIME  -   13:00
 1001                                                                 A1.24X6

 80:

 60:

 40:
                                                                           A9.74E5
                    19100               20:00               21:00               22:00
 FileiS975834 tl-848 Acq:ll-SEP-1997 12:58:11 EH- Voltage SIR  70S Noiae:30
 333.9338 Tt2 BSUB(256,30, -3. 0)  PXD(7,5,3, 0. 05\,120. 0,1. 00\,T, T) Xxp:XPCVS
 TRIANGLE LABS  ToXt:I-M23-l   TLIt43085                      IKT. TIME -   13:00
 1001
   40:

   20:

    0.
                                                                       A1.44E6
                                                                            A1.12E6
                   19:00               20:00               21:00               22:00
rile:S975834 tl-848 Acqsll-SEP-1997 12:58:11 EI+ Voltage SIR  70S NOi*e:29
327.8847 T:2 BSUB(256,30,-3.0)  PKD(7,5,3, 0. 05\,116.0,1. 00\,T, T) ExpsEPCUS
TRIANGLE LABS  Text:I-M23-l   TLI*4308S                      IKT. TIME -   13:00
1001                                                                       A1.80E6

 80:

 60:

 40:

 20:

   o< _   .-..-.-.,..         -—   -  ---  -  -
                                                                                    A9.74E4
                     19:00               20:00               21:00              22:00
  rile:S975834 tl-848 Acqtll-SEP-1997 12:58:11 EI+ Voltage SIR 70S
  330.9792 T:2 Exp:EPCOS
  TRIANGLE LABS  Text:I-M23-l   TLH43085                      IKT. TIME -   1J.-00
  1001
                           19:18          _20:06
   80J
2.4X5

1. 9E5

.1. 4E5

.9.6X4

.4.8X4
                                                                                                  0.0X0
                                                                                                     Tim
                                                                                                  2.9E5

                                                                                                  2.3E5

                                                                                                  1. 7E5

                                                                                                  1.1E5

                                                                                                  5.7X4
                                                                                                    0.0X0
                                                                                                       Tim
                                                                                                   .3.2X5

                                                                                                   .2.6X5

                                                                                                   ll.9E5

                                                                                                   .1.3X5

                                                                                                   .6.5E4
                                                                                                   0.0X0
                                                                                                      rim
                     19tOO
                                         2000
                                                             21:00
                                                                                 22 00

-------
rile, 3975834 tl-848 Aoqtll-SXP-1997 12:58:11 XI+ Voltage SIX 70S Hoite:36
339.8597 ti2 BSUX(256, 30, -3 .0 ) PXD( 7,5,3,0. 05%,144. 0,1. 00\,r,T) X*p:XPCU8
TRIANGLE LABS Text:I-M23-l 311*43085
1001
so:
60:
40:
20:
0
A1.21E5
\
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J 1 A4.51E4
I \ tal. 28*4
hVAJi. »jw trv w A. .. . -.. A.. K Ajn LJY.A
23io0 	 24i00

IHJ. TIMX - 1J.00




A6.28E3
*j'\nf}A JLA rV\jylAArJA/r
25.00



A3. 4 424
j^Ai .11 Ju ,
WwInAy'y\N\AA/''lJ\lA /
.3.0X4
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.1.2X4
.6.0X3
0.0X0
26.00 Ti*e
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341.8567 T:2 BSUB(256,30, -3 .0) PKD(7,S,3,0.05\,120.0,1.00\,T,T) Exp:EPCUS
TRIANGLX LABS Text:I-M23-l TLH43085
1001
80:
60.
40.
20.

A7.99E4

1
A1.52E4 II A2.72E4
[ A2.43X3J\ A6 25X3 J\A9-05S3
\^.fj \A_ftj_f-v**JLsjLj%«* v^*-»A* 	 A/W\^I A A rA f^ \AA-A/vA^.
23:00 24 : 00

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A vVWv A AJ\ jjpvyWUWuvV
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.2.8X4
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0.0X0
26:00 Tiae
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351.9000 T:2 BSUB(256,30r-3 .0) PKD(7,5,3, 0.05%,164. 0,1. 00\,T,T) Exp:XPCUS
TRIANGLE LABS Text:I-M23-l TLH43085
1001
80:
eo:
40:
20:
o:






'23:00 	 24.-00 '
INJ. TIME - 13:00
A9.37ES
A8.



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25:00
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2£5
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353.8970 T:2 BSUB(256, 30, -3 . 0) PKS(7, 5,3, 0. 05\,168.
TRIANGLE LABS Text: I-M23-1 TLIt43085
1001,

80'.
60.
40.
20.

0





Al . 50E4

' 23:00 	 24:00 '
0,1.00\,T,T) Exp:EPCOS

I1KT. TIME - 13:00
A6.00E5
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A A5 . 51£5
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26:00 Time
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330.9792 T:2 Xxp:EPCUS
TRIANGLE LABS TextsI-M23-l TLH43085
1003,

80.

60.
40.
20.
0

24:
_, ./v
/^ 33- 41 11.01 23:21 23:47 24:08 s^
/^\ * ^ ? * JL +j * uj ^t .. /V^y\A r




'23:00 	 24.-00 '


XK7. TIME - 13:00


26.40 ,2.2X6
"3&* 3 a A.
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'• o . oxo
26:00 ' ' ' Time
rile:S975B34 tl-848 Acqtll-SEP-1997 12.58:11 XI+ Voltage SIR 70S
409.7974 T:2 Exp:EPCUS
TRIANGLE LABS Text : I-H23-1 TLIt43085
100
80
60
40
20
0
1 24


\ 1
: | 22,53 23-153{39 34'01 34'3°
'•\,j\N(ti}( AX /AAJWA ~AA/ ^lA^^AAjsA AA-A^
23.00 24.00


TWT. TJMT » 13.00
37



25.33
JlL^M_JV\JwlMAJW _
-------
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355.8546 ft2 BSOB(256, 30,-3.0)  PXD(7,5,3,0.05\,112.0,1.00\,T,T) fzptXPCOS
TRIANGLE LABS  T*xt:I-N23-l  TLH430S5                       1X7. TIN* -   13iOO
100* Al.48X4
                                                                                                 9.3X3
         241 00                         25'tOO                          36100
 file»S975834 #1-840 Acqtll-SEP-1997 12t58:ll 11+ Voltay* SIX 70S J*>i«««3i
 357.8516 Ts3 BSUB(256,30, -3.0) PKD(7,5,3, 0.05%, 124. 0,1.00\,F,T) XrptXPCOS
 TRIANGLE LABS  T*xttI-M23-l  TLI143085                       HKT. TIME *   13tOO
 100*
         24': 00                         25:00                          26:00
 r±le:S975834 H-B48 Acqill-SEP-1997 12i58tll EI+ Voltage  SIS  70S Hoime:29
 367.8949 Tt2 BSOB(256,30,-3.0)  PKD(7,5,3,0.05\,116.0,1.00\rf,T)  XxpsXPCOS
 TRIANGLE LABS  TeittI-M23-l   TLIH30B5                       INJ. TIME -   13:00
 100\                                                                      A4.71E5
  80J

  50.

  40.

  20:
                                                                                 6.34E4
                                                                                                    0.0X0
                                                                                                       T±mi
                                                                                                  1. 6E5

                                                                                                 .1.3E5

                                                                                                 .9. 5E4

                                                                                                 .6.4S4

                                                                                                 .3.2X4
          24i00                          25:00                          26>00
 riletS975834  #1-848 Acq:ll-SEP-1997 12>58tll  XI+ Voltage SIS 70S KoiaetSl
 369.8919 T:2  BSUB(256,30,-3.0) PXD(7,5,3,0.05\,124.0,1.00\,F,T) ExpsXPCVS
 TRIANGLE LABS  Tort:I-M23-1  TLH4308S                       IXJ. TIKE  -    13»00
 100*                                                                      A3.02E5
   BO:

   eo:

   40.

   20:
                                                                                                    .0.0X0
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                                                                                .83E4
                                                                                                  9.2X4


                                                                                                  .7.3X4


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                                                                                                  '.3. 7X4


                                                                                                  '.1. 8X4
        •  i " - 'i"    i  ••• I "   i"   i •' ' "i- " "i*   -^ -  -i ' ' - -i    i      |
        34:00                          25:00                         36:00
rile.-5975834 #1-848  Acq,ll-SEP-19S7 13t58:ll EI+ Voltage  SIS 70S
330.9793 F:2 XxpsXPCOS
TRIANGLE LABS  TeztsX-«23-l   TLI#43085                       JWJ. TIME -   13:00
1001
                                                                                                    .o.oro
                                                                                                        Time
                                                                                            26:40
          34:00
                                         25:00
                                                                        26:00

-------
 ile.S975834 tl-406 Aoqill-SXP-1997 12:58:11 XI+ Voltag* SI* 70S Half•:521
 73.8208 T>3 BSUt(256,30,-3.0) PKD(7, 5,3,0.05\,2084.0,1,00\,r,T) XxpiXTCUS
TRIANGLE LABS  T*xt:I-M23-l  1X1*43085                       INJ. TIMX -   13:00

                    A3.14E4                                      *a-}"4
         27.24  27:36 27:48 28:00 28«12  28*24 28.36 28:48 25:00  29:12 29:24 29:36 29:48 JO.00  J0:12
 110:5975834 tl-406 Acq:ll-SEP-1997  12(58:11 EI+ Voltage SIX 70S No±m»:524
 75.8178 Fi3 BSUB(256,30,-3.0) PKD(7,5,3,0.05\,2096.0,1,00\,T,T) ExptEPCOS
TRIANGLE LABS  T*ztiI-M33-l  TLH43085                       IW7. TIME -   13:00
 001
                                                                                      A1.52E4
                                                                                  Al.64X4
                                                                                            A2.51X4
                                                                                                         Time
   27:12 27:24 27:36 27:48 28:00  28:12 28:24 28:36 28:48  29:00 29:12 29:24  29:36 29:48 30:00  30:12
 Tile:S975834  tl-406 Acqsll-SEP-1997 12:58:11 EI+ Voltage SIR 70S Haifa: 280
 '83.8639  r-.3  BSUB(256,30,-3 .0)  PXD(7 ,5,3,0 .05\,1120 .0,1. 00\,r,T) ExptEPCUS
 TRIANGLE  LABS  Text:X-M2J-l   TLH43085                      IKT. TIME-    13:00
                                                                                                          Timi
1003

 80:

 so:

 40:
                                             A3.52E5
                                                                A3 . 31E5
                                                                                     A3.00E5
                                                                                                    _1 . 415

                                                                                                    Ll.115

                                                                                                    .8.3E4

                                                                                                    .5 . 6E4

                                                                                                    .2.8E4
                                                                                 A9.27E3
                                                                                            tf"
                                                                                                       O.OEO
   27:12 27:24 27:36 27:48  28:00 28:12 28:24  28:36  28:48 29:00 29:12  29:24  29:36 29:48  30:00 30:12
 rile:S975834 #1-406 Acq:ll-SEP-1997 12:58:11  EI+ Voltage SIS 70S  No±ae:697
 385.8610 F:3 BSUB(256,30,-3.0) PKD(7, 5,3, 0.051,2788. 0,1. 00\,r,T)  Exp:EPCUS
 TRIANGLE LABS  Text:I-M23-1  TLIf430S5                       INJ'.  TIME -   13:00
1001

 80:

 60:

 40:

 20:

   o:
                                              A6.S1E5
                                                                A6.3SE5
                                                                                      AS.B6E5
  27:12  27:24  27:36 27:48 28:00 28.12  28:24
rile:S975834 #1-406 Acg:ll-S£P-1997 12:58:11
392.9760 F:3 Elp:EPCUS
TRIANGLE LABS   Tart:J-M23-l   TLIt43085
                                               28:36 28:48 29:00 29:12  29:24 29:36 29:48
                                               EH- Voltage SIS 70S
                                                                                                        Time



                                                                                                       .3E5

                                                                                                       .9E5

                                                                                                       .4E5

                                                                                                       .3E4

                                                                                                       .7E4

                                                                                                       .OEO
                                                                                                        Tia,
  27:12 27':24' 27': 36 27:48' 28 i 00 ' 28:12* 281-24
file:S975834 #1-406 Acq:ll-SEP-1997  12:58:11
445.7555 T:3 ExptEPCUS
TRIANGLE LABS  Text:I-M23-l  TLIt43085
1001
  I i '  i i i i	i i i i i i i i i i i i i i i i  i i i i i i i i i
28:36  26-48  29:00  29:12 29:24  29:36  29:48
EI+ Voltage SIX 70S

               INJ. TIME -   13:00
                                                                                             I  i i i i i I
                                                                                           30:00  30:12
                                                                                                        .OEO
                                                                                                         Tia
    27:12  27:24
                      27:48  28:00
                                                        _->UAWWVl/UUAA*uUl
                                                i i i i i » i ri1 r'r"i"| 'r11!11 T'T'T^TT'I i i'i i i
                                        28i24 28:36 28:48  29:00  29:12 29:24
                                      29«48 30:bb'30:12
                                                                                                         0£0
                                                                                                          Tim
                                                                                                           180

-------
\Til.,S975B34 il-401 Aogi 11-09-1997 12,58,11 KH- Voltage Sl» 70S
389.8156 Ti3 BSUB(256,30, -3.0)  PKD(7,5,3,0.05\, 1716.0,1.00\,T,T) XxptXPCaS
TXIA1KLX LABS  TeJct:I-M23-l   TLH43085                      IXT. TIMX -   13iOO
100*                                              A1.J.OX4
                                                                                               8.3X3
     27\48  ' '28\00  ' '28\12 '  '28\24  ' ' 26\36  ' ' 28\48 '  29\00   29:12    29i24   29',36\   29:48
 r±le,S975834 tl-406 Acqtll-SXP-1997 12i58ill XI+ Voltage SIS 70S Koif9,306
 391.8127 r,3 BSUB(256,30r-3.0) PXD(7,5,3,0.05\,1224.0,1.00\,r,T) XxptXPCOS
 TSIASGLX LABS  Text:I-M23-l  TLIf43085                      I1W. TIMX -   13:00
 1001
      27,48   28,00   28,12    28i24   28,36   28:48    29:00    29,12   29:24    29,36   29:48
 rile:S975834  tl-406 Acqsll-SEP-1997 12,58,11 EI+ Voltage SIS  70S «oite,316
 401.8SS8  T,3  BSUB(256,30,-3.0) PKD(7,5,3,0.05\,1264.0,1.00\,T,T) XxptSPCVS
 TXIANGLE  LABS  Taxt,I-M23-l  TLH43085                      XWJ- TIME -   JJ.-OO
  100J

   so:

   60.

   40.

   201
                                                                                   A6.12E5
                                                                    A4.43E5
                                           A1.21E4
                                                  '

2.1X5

.1. 7X5

.1. 3X5

.8.5E4

.4.3E4
    "i  i t i  i1 lO |" i1  f i-il i1         ,        ,        ,
    27,48    28,00   28,12   28:24    28:36   28:48   29:00
Tile,S975834 tl-406 Aoqill-SXP-1997 12:58:11 XI+  Voltage SIS 70S Soiae,342
403.8529 r,3 BSUB(256,30f-3 .0)  PKD(7,5,3, 0. 05\, 1368. 0,1. 00\,r,T) Xip:EPCUS
TRIANGLE LABS  Text:I-M23-1   TL.H430BS                      IKJ. TIMX  -   13:00
100*                                                                             AS. 22X5
                                                                                          29i48
                                                                                                .0.0X0
                                                                                                    Time
    ao:

    60.

    40.

    20.
                                                                 A3.15X5
         T"r
       27:48
                                          T
                                                                    A
                                                                                J
 1. 8X5

 .1.4X5

 .1.1X5

 .7.1X4

 .3. 6X4
            28:00    28:12   28:24    28:36   28:48   29,00   29tl2    29,24   29:36
Tile,S975834 tl-406 Acqill-SEP-1997 12:58:11 EH- Voltage SIS 70S
392.9760 T,3 Xxp:EPCUS
TRIANGLE LABS  Text:I-M23-l  TLIt43085                      J*J- TIMX -    13:00
                                                                                        29,48
                                                                                                 .0.020
                                                                                                     Time
   1001

    so:

    60.

    40.

    20.
       27:52
                            28:21
                                     28:34
                                                 28,52"'°°
                                                                        29:26
                                                                                29:33
 _.! . 8X6

 .1.4X6

 .1.1X6

 '.7.2X5

 .3.6X5

" t 1 1 1 1 1
27,48

'28160 ' ~28i

12 28\24

28:36

26,48

29 1 00 29 1

12 29:24 29

i 36 29\48
.0.0X0
fH
                                                                                                              18

-------
 ile:S975834 tl-430 Aoqill-SXP-1997 13i58tll  II* Voltage SIM 70S Nolle:1774
 07.7818 Ti4 BSUB(256,30,-3.0) PXD(7,5,3,0.05\,7096.0,1.00\,r,T) XxpiXPCOS
TXIANCLS LABS  Text:I-M23-l  TLH43085                       IKT. TIM* -   13iOO
 001
                                31:36     31i48      33.00      32s 12     32i24
 ile:S975834 #1-430 Acqill-SEP-1997 12:58:11 EH- Voltage SIX 70S Koi»e:1037
 09.7789 T:4 BSUS(256,30,-3.0)  PKD(7,5,3, 0.05*, 4148.0,1.00\,F,T) XxptEPCUS
TRIANGLE LABS  Text:I-H23-1  TLH43085                      INJT. TIME  -   13:00
100*
 80J         '                                                       A2.06E4

 sol
 40:

 20:.

   0:
                                                                                    32136
                                                                                              32:48
           31:12      31:24     31:36     31:48      32:00     32:12      32:24
Tile:S975834  tl-430 Acg_:ll-SEP-1997 12:58:11 EH- Voltage SIS  70S Noime:690
  17.8253 F:4  BSUB(256, 30, -3. 0) PKD(7,5,3,0.05\,2760.0,1.00\,F,T) XxptXPCOS
TRIANGLE LABS  Text:I-M23-l  TLH43085                      I1KT. TIME -   13tOO
1001             A1.70E5
                                                                                    32:36
                                                                                               32:48
  40

  20:

   0:
                                                                              A1.49E5
                            Al.02E4
                                         Al.19X4
                                                                                       A^-^^V J^^^^\.^N-i
                                                                                                     9.6X3

                                                                                                      7.7X3

                                                                                                     .5.8X3

                                                                                                      3. 8X3

                                                                                                     ,1.9X3

                                                                                                     ,0.0X0
                                                                                                         Time



                                                                                                     .4.7X4

                                                                                                     .3. 8X4

                                                                                                     .2.8X4

                                                                                                     .1.9X4

                                                                                                     .9. 5X3
            31il2     31:24     31:36      31:48     32:00     32:12      32:24
 F±le:S975834 il-430 Acq:ll-SEP-1997 12:58:11  EH-  Voltage SIX 70S Jtoi«e:701
 419.8220 T:4 BSUB(256, 30, -3. 0) PXD( 7,5,3, 0. 05\,2804. 0,1. 00\,T, T) XxpsXPCUS
 TRIANGLE LABS  Text; I-M23-1  TLH43085                       JK7. TIME -   IJtOO
                                                                                   32:36
                                                                                              32:48
1003


 60:

 40:
 20:
  0:
                 A3.93E5
                                                                               A3.28X5
                                                                                         A1.34E4
                                                                                        ^-^|__-^v_".jfc^ ^*r~*.^
           31:12     31:24      31:36     31:48     32tOO      32:12
rile:S975834 fl-430 Acqtll-SXP-1997  12:58:11 EI+ Voltage SIX 70S
430.9729 Ts4 ExpsEPCUS
TRIANGLE LABS  TexttI-M23-l  TLIt43085                      HTJT. TIME
                                                                          32:24
                                                                                     32136
                                                                                               32:48
       O.OEO
          Tim.
       1.0X5

       8.4X4

       6.3X4

       4.2X4

       2.1X4

       0.0X0
           Time
                                                                            13:00
1003
 80:
 60:
 40:
 20:
   o:
               31:15
                                                    31:58 32:05
                                                                                      32:3732:43
              -r
                        -r
                                                                  T
                                                                           32:24
           31:12      31:24     31:36     31:48      32:00     32:12
File:S975834 fl-430 Acq:ll-SEP-1997 12:58:11 EI+ Voltage SIX  70S
479.7165 T:4 EiptEPCUS
TXIANGLE LABS  Text:I-M23-l   TLIH43085                      IHJ. TIME -   13s00
                                                   31; 57
                                                                                     32:36
32\4B
        1. 8X6

       .1.5X6

       .1.1X6

       '-7.4X5

       .3. 7X5
0.0X0
   Tim
            31.1.2
                       31124
                                 31136
                                            31:48
                                                      32:00
                                                                32 > 12
                                                                                               32:48
                                                                                                      0.0X0
                                                                                                          Tim
                                                                                                             182

-------
      17:00           18:00           19:00           20»00           21:00
 ile:S975834 91-848 Acqsll-SXP-1997 12>5Bill EI+ Voltage SIX  70S Jfciae.347
 05.8987 Ts2 BSUB(256,30,-3.0) PKD(9, 5,5,0.05\, 1388.0,1.QO\,T,T) ExptEPCUS
TRIANGLE LABS  Text:I-M23-1  TLH43085                      IKT. TIME  -  13:00
      17:00           18:00           19:00           20:00           51:00
Tile:S975B34 #1-848 Acq:ll-SEP-1997 12:58:11 Eli- Voltage SIS  70S Noif»:39
 15.9419 T:2 BSUB(256,30, -3. 0) PKD(9,5,5, 0. 05\,156. 0,1.00\,T, T)  ExptEPCUS
TRIANGLE LABS  Tert:I-M23-1  TLH43085                      INJ. TIHX -   13:00
 004                                                                  Al. 09E6

 sol

 so:

 40:

 20.
 ilei5975834  #1-848 Acqtll-SXP-1997  12:58:11  XI+ Voltage SIX 70S Koime:99
 03.9016 f:2  JSSU*(256,3Q,-3.0)  PKD(9 , 5 ,5,0 .05\,396 .0 ,1.00\,T,T) XxpiXTCUS
  lANSLf LABS  Text:I-M23-1  TLH43085                      IJKT. TIHX -   13:00
 001                                 s^y   A7.55X4
                                                                                                       «*•
                                                                                    32100
                                                                                    221 00
                             ore
                              Time



                           2.1X5

                           ,1. 6E5

                           1.2X5

                           .8.2S4

                           .4.1X4
      17:00           18:00           19:00           20:00           21:00
 •ile:S975834 #1-848 Acq:ll-SEP-1997  12:58:11  EI+ Voltage SIX 70S Noiae:34
 17.9389 T:2 BSOB(256,30,-3.0)  PKD(9,5,5r0.05\,136.0,1.00\,reT) Exp:£PCUS
TRIANGLE LABS  TextsI-M23-1   TLH43085                       I1W. TIHX -   13:00
                                                                                     22:00
                                                                                                     O.OEO
                                                                                                        Tine
 100J

  80:

  50J

  40:

  20:

   0.
                                                                       A1.4BE6
      17:00           18:00           19:00           20:00           21:00
file:S975834 #1-848 Acg:ll-SEJ>-1997 12:58:11 EH- Voltage  SIS 70S
330.9792 T:2 ExpsEPCUS
TRIANGLE LABS  T*xtsI-H23-l  TLH43085                       INJ. TIHE -   13:00

         17:11
 80:

 50:

 40:

 20J

   0.
                                                                                      22:00
                                                                                                     P--1-
                                                                                                     _1.

                                                                                                     Li.

                                                                                                     .6,

                                                                                                     .3
       17:00            18:00           19:00           20:00           21:00
 Tile:S97S834 #1-848 Acgr:ll-Si;j'-1997 12:58:11 EH- Voltage  SIS 70S
 375.8364 T:2 Exp:XPCUS
 TSIANGLE LABS  TejctsI-H23-l  311 #43085                       OU.  TIHX -   13:00

                     17:53
                                                                                      22:00
  80:

  60l

  40:

  20:
         17:10
               17.35I
                              18:28
                                           ""
-••"        »«         •
                             2E5

                             .6X5

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                             .0X0
                              Tim



                             .7E6

                             4E6

                             OE6

                             8X5

                             4X5

                            J.OEO
                               Time



                            1.1E4

                            3.5X3

                            S.4X3

                            t.3X3
       17100
                       18:00
                                       19:00
                                                      20:00
                                                                      31100
                                                                                      22100
                                                                                                       i.oro
                                                                                                         TlMJ
                                                                                                            is:

-------
\H1»:S975B34 U-430 Xoq:ll-SSP-lS97 12,5V< 11  XH- Voltage 311 70S Hbi«««6*7
423.7766 r:4 3SVS(256,30,-3.0) PKD(7,5,3,0.05\,2668.0,1.00\,r,T) XxpiXPCOS
TXIJUKLX LASS  Tmxt:I-M23-l  TLH43085                       IHJ. TIMS -   13iOO
10(A                    A3.56X4
80.

60.

40.

20.
       A2.05X3
                                   T
                                          T
                                                 -r
                                                        T
                                                            '32\06 ' '32', 12 ' '32', 18
     3lil«  31', 24  31', 30  31', 36  31:42  31:48   31,54   32,00
 Tlle:S975834 tl-430 Acqill-SEP-1997 12,58,11 XI+ VoltMgm  SIX 70S Koimti401
 425.7737 Ti4 BSOB(256,30,-3.0) PXD(7,5,3,0.05\,1604.0,1.00\,T,T) XxpiXPCOS
 TRIASGLX LABS  T*xtil-l423-l  TLH430B5                       IJKT. TIKE -   13100
 IOCS                   A4.P7E4

  80.
                                                                                   '32',24 ' 32', 30
                                                                                                .9.2X3

                                                                                                .7.3X3

                                                                                                '.5.5X3

                                                                                                .3.7X3

                                                                                                .1. 8X3

                                                                                                 0.0X0
    31:18  31:24  31:30  31:36  31:42   31:48   31:54  32:00 ' 32:05  32:12  32:18
T±le:S975834 tl-430 Ac
-------
file:5975834 tl-430 Aoqill-SEP-1997 12:58:11 EI+ Voltag* SIM 70S tfoif«t3l
441.7428 T>4 BSU*(25f,30,-3.0) PtX>(7, 5,3,0,05\, 124.0,1.00\efrT) XxptXTCOS
TRIANGLE LASS  T*xttI-K23-l  ZU 443065                       XK7. TJMT -   13iOO
1003
          31': 00             32,00             33iOO             34tOO
 rile:S975834 tl-430 Acqtll-SEP-1997 12s58-.11 EI+ Voltage SIX  70S J*oi*e:28
 443.7399 T:4 3SUS(256,30,-3.Q) PKD(7,5,3, 0. 05%, 112. 0,1. 00\,r,T) XxptXPCOS
                                                                                35:00
                                                                                                         Tim*
 TXIANGLE LABS
 1003.
                Tezt:X-M2J-l  TLH43085
                                                             XKT.  TIKX -   13:00
          31': 00             32:00             33': 00             34:00             35:00
 rile>S975634 tl-430 Ac'a* "!4B
                                                    33:20
XWJ. TIME -   13:00
      34:14  34(3B
  34:02 ,
                                                                                     35:12
                                                                                                35:48 r
          31:00             32:00             33:00             34:00             35:00
 file.-5975834  41-430 Acq:ll-SEP-1997 12:58:11 EI+ Voltage SIS  70S
 513.6775 Tt4  Exp:EPCUS
 TRIANGLE LASS  Tart.-I-W23-1  TLI#43085                      INJ.  TIME -   13:00
                                                                                                       1.9E6
                                                                                                       1.6E6
                                                                                                       1.4X6
                                                                                                       1.2E6
                                                                                                       1. OE6
                                                                                                       .8.2E5
                                                                                                       6.2X5
                                                                                                       .4.1X5
                                                                                                       2.1E5
                                                                                                       iO.OEO
                                                                                                           Tim
           31 i 00
                             32:00
                                              33iOO
                                                               34:00
                                                                                 35:00
                                                                                                            18

-------
\ril»:S975834 tl-430 Aoq:ll-SXP-1997 12>58ill  XH- Voltage SIS 70S J*oi»e«J«
\457.7377 Ti4 BSUB(256, 30,-3.0) PKD(7, 5,3,0.05\, 136.0,1.00\,F,T) XxptXPCOS
TRIANGLE LABS  TvctiI-H23-l  1X1*0085                       1X7. TIHX •   13tOO
100\                                             A4.26X5

  so:

  SO.

  40.

  20.
                                                                                             -5.9X4

                                                                                              .4.7X4

                                                                                              .3.5X4

                                                                                              .2.3X4

                                                                                              .1.2X4
       34,24        34,30         34:36         34,42         34,48         34,54
 rile:S975834  tl-430 Acqtll-SXP-1997 12,58,11 XI+ Voltage SIX  70S  Ho±ee:31
 459.7348 T:4  BSUB(256,30,-3.0) PXB(7,5,3, 0.05%, 124.0,1. 00\,r, T) Xzp:XPCVS
 TXIAKGLX LABS  Text.J-M23-1  TLH4308S                      IXT.  TIHX -   13,00
                                                                                          35100
                                                                                                  .0. 0X0
                                                                                                     Time
 1003

  80.

  60.

  40:

  20.
                                                       A4.59X5
                  i  i  i  "i  i '
                  34,30
                                                                                              -5.6X4

                                                                                              .4.5X4

                                                                                              .3.4X4

                                                                                              .2.3X4

                                                                                              .1.1X4
                                  i   r i   i  T  i  i   i  i  i   i  i  i  i   .....  ii
       34,24         34,30        34,36         34,42         34,48         34,54
 rile,S975834 tl-430 Acqill-SEP-1997  12,58:11 XI+  Voltage SIX 70S Noiae:26
 469.7779 T,4 BSOB(256, 30, -3. 0) PKD( 7,5,3, 0.05\,104. 0,1. 00\,F, T)  XxpiXPCUS
 TRIANGLE LABS  Texts I-M23-1  TLH43085                       INJ. TIHX -   13:00
 1001                                                  A2.89E5
.0.0X0
    Time
        34:24         34:30         34:36         34:42         34,48         34:54
  T±le,S975834  tl-430 Acq:ll-SEP-1997 12:58:11 EH- Voltage SIB 70S Noiae:286
  471.7750  r,4  BSUB(256,30,-3.0) PKD(7,5,3, 0. 05\,1144 . 0,1. 00%,T,T) Exp:EPCOS
  TRIANGLE  LABS  Text:I-H23-l  TLH430BS                      JKT. TIMX-   13:00
  1004                                              A3.68E5
so:
eo:
40:
20:
                                                                                          35:00
                       A7.63E3
                                                                                                   5.0X4

                                                                                                  .4. 0X4

                                                                                                  .3. 0X4

                                                                                                  .2.0X4

                                                                                                  .1. 0X4


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430.
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1003

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40_
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34\24 '34\3Q ' ' ' 34\ 36 ' ' ' ~34\42 ' ' ' 34\48 ' ' ' '34^54 ' ' ' 3s':00
,3975834 tl-430 Acq,ll-SEP-1997 12:58:11 EI+ Voltage SIX 70S
9729 T:4 ExpsXPCUS
HGLE LABS Text: I-M23-1 TLH43085 IKJ. TIHX - 1J.-00
34:38
34,28 ^ \X^^ J2^1~^ 	 ^/-\
^^ ~^^^ N/ ^^ " *~^~*^S~




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Time



.2.1X6

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.4.1X5
0.0X0
Time
                                                                                                           186

-------

-------
•-ile:S975834 #1-430 Acq:ll-SEP-1997  12:58:11 EI+  Voltage SIR 70S
117.8253 F:4 Exp:EPCUS
Sample Text:I-M23-l  TLI#43085
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119.8220 F:4 Exp:EPCUS
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-------
File:S975834  #1-430 Acq:ll-SEP-1997 12:5ft:ll EI+  Voltage  SIR  70S
423.7766  F:4  Exp:EPCUS
Sample Text:I-M23-l  TLI#43085                       INJ.  TIME =
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File:S9Vb834 #1-430 Acq: ll-SEP
423.7766 F:4 Exp: EPCUS
Sample Text:I-M23-l  TLI#43085
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^ile:S975834  #1-430 Acq:ll-SEP-199712758~TTr^EI+ Voltage SIR  70S	
157.7377 F:4  Exp:EPCUS
Sample Text:I-M23~l  TLI#43085,                      INJ. TIME =    13:00  File Text:I-M23-l  TLI#»
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:'ile:S975834 #1-430 Acq: ll-SEP-1997  12:58:11 EI+ Voltage SIR 70S
159.7348 F:4 Exp:EPCUS
Sample Text:I-M23-l  TLI#43085                       INJ. TIME =    13:00  File Text:I-M23-l  TLI#»
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?ile:S975834 #1-430 Acq:ll-SEP-1997 12:58:11  EI+  Voltage SIR 70S
169.7779 F:4 Exp:EPCUS
Sample Text:I-M23-l  TLI#43085                       INJ. TIME =   13:00 File Text:I-M23-l  TLI#»
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                                                                                Time
        31:00           32:00            33:00            34:00
•'ile:S975834 #1-430 Acq: ll-SEP-1997 12:58:11  EI+  Voltage SIR 70S
171.7750 F:4 Exp:EPCUS
Sample Text:I-M23-l  TLI#43085                       INJ. TIME =   13:00 File Text:I-M23-l  TLI#»
LOOSi                                                                34:44                   5. OE4

                                                                      ll.
                                                                                           12.5E4

                                                                                            O.OEO
        31:00           32:00            33:00            34:00           35:00                  Time
30:45 31:19 32:07 33
A
:01 33:40 34:06 34:3/ \ 35:12 35^4
A^^^~=vst^^^v^>-^^^<^^/v^~^uV'A•s/y'xv~^A^v> — r^v

-------
7ile:S975834 #1-430 Acq:ll-SEP-1997 12:58:11 EI+ Voltage SIR 70S
169.7779 F:4 Exp:EPCUS
Sample Text:I-M23-1  TLI#43085
100%
                                         INJ.  TIME  =    13:00  File Text:I-M23-l  TLI#>
                                                     INJ. TIME =
                                        33:00           34:00
>ile:S975834 #1-430 Acq:ll-SEP-1997  12:58:11 EI+ Voltage SIR 70S
171.7750  F:4 Exp:EPCUS
Jarople  Text:I-M23-l  TLI#43085
LOO*
 90 j
 80 j
 70 J
 60 J
 50J
 40J
 30J
 20 J
                                                      13:00 File Text
                                                      34 44
                           :I-M23-1  TLI#»
 10J
  0.
    30:45
31:19
                          32:07
                                        33:01
    '< ' '   I	r
       31:00
                   31:42 I ,  I    32:31 A    I      AA33i4?
                   v^XvxvJuAJK^^v^N^AAAA/^ W-^AJu>A^w^uwW^Jvwky\
                        32:00
                           33:00
34loo'
"ssloo

-------
TLI Project:      43085
Client Sample:   I-M23-2
Method 23 PCDD/PCDF Analysis (a)
             Analysis File:  S975835
Client Project:
Sample Matrix:
TLI ID:

Sample Size:
Dry Weight:
GC Column:
S413-004
M23Train
181-55-6ABD

1.000
n/a
DB-5

Date Received:
Date Extracted:
Date Analyzed:
Dilution Factor:
Blank File:
Analyst:

09/03/97
09/04/97
09/11/97
n/a
S975815
BJG

Spike File:
ICal:
ConCal:
% Moisture:
% Lipid:
% Solids:

SPX23704
SF56117
S975814
n/a
n/a
n/a
Analytes ;
2,3,7,8-TCDD
1,2,3,7,8-PeCDD
1, 2,3,4 ,7,8-HxCDD
1,2,3,6,7,8-HxCDD
1,2,3,7,8,9-HxCDD
1,2,3,4.6,7.8-HpCDD
1,2,3,4,6,7,8,9-OCDD
2,3,7,8-TCDF
1,2,3,7.8-PeCDF
2,3,4,7,8-PeCDF
1,2,3,4,7,8-HxCDF
1.2,3,6,7,8-HxCDF
2,3,4,6,7,8-HxCDF
1,2,3,7.8,9-HxCDF
1.2,3,4,6,7,8-HpCDF
1,2,3,4,7,8,9-HpCDF
1,2,3,4,6,7,8,9-OCDF

•Totate .- •• . ^i.!"
Total TCDD
Total PeCDD
Total HxCDD
Total HpCDD
Total TCDF
Total PeCDF
Total HxCDF
Total HpCDF
Amt (ng)
ND
ND
ND
ND
ND
1 ^Ls
ND
8.2
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND

'/••:v4:;':-''f:;':Amtr. (rig)
ND
ND
ND
ND
0.17
0.33
ND
FJvlPC
DL EMPC
0.03
0.06
0 1
\J . 1
0.09
0 f)0
V/.V/^'
0.2

0.02
0.04
0.04
0.06
0.05
0.06
0.07
0.1
0.1
04
\J .^
Number DL EMPC
0.03
0.06
0.10
0.2
2
1 0.47
0.06
0.26
Ratio at ^ ftcgr


~
—
~~~~*
—
0.82 34:42 ~











Ftegs



	




                                        Page 1 of 2
                                                                         X237 J>SR YlOO, LARS 6.10 04
Triangle Laboratories, Inc.®
801 Capitola Drive • Durham, North Carolina 27713
Phone: (919) 544-5729 • Fax: (919) 544-5491
                       Printed: 15:2600/1

-------
TLI Project:      43085
Client Sample:   I-M23-2
Method 23 PCDD/PCDF Analysis (a)
             Analysis File:   S975835
lntematS«ard«-.3myf
3C.2-2,3,7,8-TCDF
13C,2-2,3,7,8-TCDD
13C,2-l,2,3,7,8-PeCDF
13C,2-l,2,3,7,8-PeCDD
13C,2-l,2,3,6,7,8-HxCDF
13C,2-l,2,3,6,7,8-HxCDD
13CP.-l,2,3,4,6,7,8-HpCDF
13Cp-l,2,3,4,6,7,8-HpCDD
13Cu-l,2,3,4,6,7,8,9-OCDD

Surrogate Standards {Type A)
37CL,-2,3,7,8-TCDD
l3C,:-2,3,4,7,8-PeCDF
13Ci:-l,2,3,4,7,8-HxCDF
13Cp-l,2,3,4,7,8-HxCDD
13Ci2-l,2,3,4,7,8,9-HpCDF

Alternate Standards (Type A)
13Cp-l,2,3,7,8,9-HxCDF
13C,2-2,3,4,6,7,8-HxCDF
. Recovery Standards -.'v:/;'-. :N ••';.:
13Ci2-l,2,3,4-TCDD
13Cii-l,2,3,7,8,9-HxCDD
Amt (ngj
1.8
2.0
1.4
1.4
2.3
2.0
1.3
1.2
14

Amt. (ng)
4.1
3.5
4.0
36
34

.;. Arnt. :(ng)
20
2.2


% Recovery
45.4
50.6
36.1
35.5
569
49.5
32.2
30.0
17 5

'•" • :: % Recovery
102
87.4
100
902
843

^•m^F^wyl
49 9
53.8
" '. -:•"..: !:x' '••'•:'::.:^::::C ;. '•' ' ' "•' '.'.'.

QC Limits
40%- 130%
40%- 1 30%
40%- 130%
40%- 130%
40%-130%
40%- 130%
25%-130%
25%- 130%
25%- 130%

QC Limits
70%- 140%
70%- 140%
70%- 140%
70%- 140%
70% -140%

jit- QC Limits
40% -1 30%
40%- 130%
<

Ratio
0.77
0.81
1.55
1.40
048
1.21
0.49
1 03
080

Ratio :
1.43
0.52
1 32
042

r:- Ratio "14
0 SA
0.51
Ratio
0.83
1.18
«T
20:44
21:30
24:54
26:01
28'35
29:18
31:16
32-07
34-42

RT
21:31
25:39
28:29
->9- 13
32-28

":"^RT ;-
">9-47
29:05
RT
21:17
29:35
Flags
v,ol_
v,Q_
_-
N

Flags
—
R

."•••Flags. '

—
Flags
—
                      Data Reviewer
                                        Page 2 of 2
             09/18/97
                                                                          X237.PSR vXOO. LARS 6.10.0*
 Triangle Laboratories, Inc.®
 801 Capitals Drive • Durham, North Carolina 27713
 Phone: (919) 544-5729 • Fax: (919) 544-5491
                       Printed: 15:26 09/1
134

-------
Data Review By:
                      Initial   ....Date...
                       CU
                                ''I  / 10 /If
                                            Calculated Noise Area:
The Total Area for each peak with an ion abundance ratio outside
ratio limits has been  recalculated according to method requirements.
                                                                   1.49
Page No.
09/18/97
                       Listing of S975835B.db£
                       Matched GC Peaks  / Ratio / Ret. Time
Compound/
M_2....  OC.Log Omit Why ..RT. OK .Ratio Total.Area... Area.Peak.1.. Area.Peak.2..  Rel.RT Compound.Name..  ID..  Flags.
TCDF
304-306

D
D

D
D

304-306
13C12-TCDF
316-318







316-318
TCDD
320-322
D













320-322
0. 65-0.89
DC

DC
DC

DC
DC
DC


DC
DC
DC
DC
DC
DC
DC



DC
DC
DC
DC
DC
DC
DC
DC
DC
DC
DC
DC
DC
DC
DC

NL

SN
SN

SN
SN
SN
2

NL
WL
WL
WL
WL
WL
SN

1

NL
SN
SN
SN
SN
SN
SN
SN
SN
SN
SN
SN
SN
SN
SN
0
0:
18:
18:
18:
19:
19:
20:
21:
00
04
27
49
08
35
46
27
RO

RO


RO
RO
RO
6.
0.
1.
0.
0.
1.
1.
5.
00
66
41
33
76
07
35
30
Peaks

0:
16:
17:
17:
18:
19:
20:
20:

00
46
25
47
19
00
15
44
0.


RO

RO
RO
RO

0.
11.
2.
14.
16.
8.
5.
0.
28.
11
92 4.72
62
14
17 6.99
50
40
71
09
65-0.89
0.
0.
0.
0.
86
86
29
72
0.52
1 .
35
0.21
0.
Peak

0
18
18
19
19
19
20
20
20
21
21
22
22
22
22

:00
:42
:51
:06
:26
:52
:15
:34
:55
:32
:53
:02
:19
:31
:43
0.

RO
RO
RO
RO

RO
RO
RO

RO
RO

RO
RO
.77

0.
1.
0.
1.
13
64
87
82
1.15
2.07
1 .
518.
.63
.30 226.11
0.820-
0.
7.20 0.
0.
0.
9.18 0.
0.
1.
1.

1.101
000
871
890
908
923
945
002 2378-TCDF AN
035

0.951-1.049
0.
0.
0.
0.
0.
0.
0.
292.19 1.
000
309
340
358
383
916
977
,000 13C12-2378-TCDF ISO
518.30
m/*r\^ / »wr\r\ c>«*i i .*...«.
65-0.89
0
1
1
1
1
0
0
0
4
0
0
2
0
0
1
.86
.01
.02
.49
.21
.72
.48
.38
.00
.77
.45
.10
.89
.61
.45
Peaks
0
2
0
1
0
0
1
0
0
1
1
0
1

.13
.19
.30
.96
.51
.62
.47
.46
.50
.47
.08
.35
.40
0.90
1
.19
0.853-1.059
0
0
0
0
0
0
0
0
0
1
1
1
1
1
1
.000
.870
.877
.888
.904
.924
.942
.957
.973
.002 2378-TCDD AN
.018
.025
.038
.047
.057
0.00
 37C1-TCDD
 328
                DC  NL   0:00
                                              0.05
                                                                           0.906-1.094
                                                                              0.000
 Triangle Laboratories, Inc.® Analytical Services Division
 801 Capitola Drive • Durham, North Carolina 27713
 Phone: (919) 544-5729 • Fax: (919) 544-5491
                                                                                            Printed: 15:1908/18&
                                                                                                          19*

-------
 Page No.

 09/18/97
Listing of S975835B.dbf
Matched GC Peaks / Ratio  / Ret. Time
 Compound/

 M_Z....  QC.Log Omit Why ..RT. OK Ratio Total.Area... Area.Peak.1.. Area.Peak.2.. Rel.RT Compound.Name.. ID.. Flags.
DC
DC
DC
DC
DC
DC
DC
DC
DC
DC
DC
DC
DC
DC
DC
DC
328
13C12-TCDD
332-334 DC
DC
DC
DC
DC
DC
DC
DC
DC
DC



DC
DC
DC
332-334
PeCDF
340-342 DC
DC

DC
DC

DC
D DC
WL
WL
WL
WL
WL
WL
SN
SN
SN
3N
SN
SN
SN
SN
SN
SN
3

NL
WL
WL
WL
WL
3N
SN
SN
SN
SN



SN
SN
SN
4
NL
WL

SN
SN

SN
SN
18:
18:
18:
18:
19:
19:
19:
20:
20:
20:
21:
21:
21:
21:
21:
22:
22.
22:
22:
Pee

0:
18:
18;
19:
19:
20:
20:
20:
20:
20:
21:
21:
21:
22:
22:
22:
22:
Pef
0:
22:
22;
23;
23;
24;
24:
24:
05
43
46
55
03
08
54
10
25
46
02
15
31
39
53
19
26
33
41
iks

00
11
43
14
23
13
16
23
35
39
17
30
50
03
21
:26
:48
iks
i 00
;36
:'>2
;14
;38
;03
:12
;32

0.
RO
RO
RO
RO
RO
RO
RO
RO
RO
RO


RO
RO
RO
RO
RO
1 .
RO
RO

RO
RO
RO
RO


65
26
3
0
2
1
2
1
1
2
3
0
0
1
1
10
1
2
32
0
0
1
0
2
1
0
1

-0.89
.43
.23
.59
.70
.61
.64
.94
.07
.37
.67
.83
.81
.23
. 34
. 30
.70
.01
1
-1 .78
.16
.34
.63
.70
.50
.24
.11
.46
1.
0.
0.
0.
0.
0.
108.
0.
0.
0.
0.
0.
403.
0.
11.
0.
1.
0.
1.
522.

0.
1.
1.
1.
1.
1.
1 .
0.
0.
0.
866,
467.
8.
1.
0.
0,
3.
.346.
Tr*nT
1 <— Ul
0.
0,
33,
0.
0.
13,
0,
4,
58
41
45
41
39
30
61 108.61
75
55
99
95
24
20 403.20
95
07 11.07
78
12
61
01
88

12
.43
59
40
96
75
95
99
,90
58
,86 392.91
,44 208.59
94 6.21
.24
,81
,89
.33 3.77
,57
.12
,43
.00 20.47
.77
.71
.18 8.01
.25
.92
0
0
0
0
0
0
0
0
0
0
0
0
1
1
1
1
1
1
1
0.906
0
0
0
0
0
0
0
0
0
0
473.95 0
258.85 1
5.05 1
1
1
1
1.88 1
0.907
0
0
12.53 0
0
0
6.48 0
0
0
.841
.871
.873
.880
.886
.890
.926
.938
.950
.966
.978
.988
.001 37C1-TCDD SUR1
.007
.018
.038
.043
.049
.055
-1.094
.000
.346
.871
.895
. 902
.940
.943
.952
.957
. 960
.990 13C12-1234-TCDD RSI
.000 13C12-2378-TCDD IS1
.016
.026
.040
.043
.060
-1.078
.000
.901
.912
.926
.942
.959
.965
. 97R
Triangle Laboratories, Inc.® Analytical Services Division
801 Capitola Drive • Durham, North Carolina 27713
Phone: (919) 544-5729 • Fax: (919) 544-5491
                                                                   Printed: 15:19 09/1^6

-------
Page No.
09/18/97
Listing  of S975835B.dbf
Hatched  GC Peaks / Ratio  / Ret. Time
Compound/
M_Z....  QC.Log omit why ..RT. OK Ratio Total.Area... Area.Peak.1.. Area.Peak.2.. Rel.RT Compound.Name.. ID..  Flags.
D
340-342
13C12-PeCDF
352-354



N
N

N


352-354

PeCDD
356-358






356-358
13C12-PeCDD
368-370




N
N

368-370

HxCDF
374-376
D
D

D
DC
DC
DC
DC
DC
DC

DC
DC
DC
DC

DC



DC



DC
DC
DC
DC
DC
DC
DC


DC
DC
DC
DC
DC


DC



DC
DC
DC
DC
DC
SN :
SN :
SN :
SN :
SN
SN
2

NL
SN
SN
SN

SN



SN
4


NL
WL
SN
SN
SN
SN
SN
0

NL
SN
SN
SN
SN


SN
2


NL
SN
SN
SN
SN
24:49 RO
25:15 RO
25:23 RO
25:27 RO
25:51 RO
26:45 RO
Peaks
1.2
0:00 RO
22:44 RO
23:04 RO
23:19 RO
24:54
25:05
25:10 RO
25:39
25:56 RO
26:38 RO
Peaks

1.
0:00 RO
24:00 RO
24:09 RO
24:21 RO
26:00 RO
26:18 RO
26:34
Peaks
1.
0:00 RO
23:56 RO
24:20 RO
25:28 RO
25:42 RO
26:01
26:08 RO
26:51 RO
Peaks

1
0:00
27:38
28:08
28:26 RO
28:34 RO
2.45
0.29
3.72
0.44
2.31
0.56
12-1.78
0.86
0.39
2.23
0.84
1.55
1.35
1.26
1.43
1.06
1.07


32-1.78
1.00
2.33
2.59
0.53
1.12
0.78
1.49

32-1.78
1.20
0.56
0.89
0.66
0.60
1.40
1.12
1.96


.05-1.43
1.09
1.24
1.43
4.69
0.79
1.02
1.48
0.74
1.53
5.61
1.65
46.18

0.10
0.94
1.22
1.69
354.68 215.73
2.09
3.08 1.87
300.59 177.02
2.50 1.52
1.66
660.85


0.12
2.07
1.76
1.41
1.50
0.41
2.32
0.00

0.10
1.02
0.64
0.94
0.20
195.33 114.11
19.63 11.93
2.40
214.96
D»fTM"\ I UvrTM? T?*-il 1 i-ibf«
i rSt-ULJ / ttX\_iM'r r ox .LOWS — — •
2.65
6.48
3.92
1.10
2.47
0.989
1.007
1.012
1.015
1.031 23478-PeCDF
1.066
0.838-1.162
0.000
0.906
0.920
0.930
138.95 0.993 13C12-PeCDF 123
1.000
1.49 1.003
123.57 1.023 13C12-P6CDF 234
1.43 1.034
1.062


0.921-1.026
0.000
0.918
0.924
0.932
0.995
1.006
1.017

0.845-1.155
0.000
0.916
0.931
0.974
0.983
81.22 0.996 13C12-PeCDD 123
10.61 1.000
1 .027


0.955-1.052
0.000
0.967
0.984
0.995
0.999 123678-HxCDF
KN





IS2.


SUR2



















IS3









AN
 Triangle Laboratories, Inc.® Analytical Services Division
 801 Capitola Drive • Durham, North Carolina 27713
 Phone: (919) 544-5729 • Fax: (919) 544-5491
                                                                     Printed: 15:

-------
Page No.
09/18/97
Listing of  S975835B.db£
Matched GC  Peaks / Ratio / R«t. Tin*
Coirpound/
M_Z.... QC.Log Omit  Why  ..RT. OX Ratio Total.Area...  Area.Peak.1..  Area.Peak.2..  Rel.RT Compound.Name..  ID.. Flags.

D





374-376
13C12-HXCDF
384-386













334-386
HxCDD
390-392
D











390-392
13C12-HXCDD
402-404




DC
DC
DC
DC
DC
DC
DC
DC
DC


DC
DC
DC
DC
DC
DC
DC
DC
DC



DC



DC
DC
DC
DC
DC
DC
DC
DC
DC
DC
DC
DC
DC


DC
DC
DC
DC
DC
SN 29:10
SN 29:17 RO
SN 29:19
SN
SN
SN
SN
SN
WH
0

NL
SN
SN
SN
SN
SN
SN
SN
SN



SN

4

NL
SN
SN
SN
SN
SN
SN
SN
SN
SN
SN
SN
WH
0

NL
WL
WL
WL
WL
29:30
29:38
29:41
29:47
30:02
30:08
Peaks

0:00
27:13
27:17
27:25
27:30
27:49
27:54
28:05
28:22
28:29
28:35
29:05
29:34
29:47
Peaks

0:00
28:02
28:14
28:30
28:31
28:42
28:46
29:03
29:10
29:14
29:19
29:34
29:49
Peaks

0:00
27:47
27:57
28:00
28:07

RO
RO
RO
RO
RO

0.
RO
RO
RO
RO
RO
RO

RO
RO



RO


1 .

RO
RO
RO
RO
RO
RO
RO
RO
RO
RO
RO
RO

1
RO
RO
RO
RO
RO
1.16
0.29
1.24
1.
0.
5.
0.
1.
0.

43-
0.
0.
3.
0.
0.
0.
0.
2.
1 .
0.
0.
0.
2.
0.

12
37
42
26
62
34

0.59
69
85
74
62
83
94
48
05
84
52
48
51
.40
.54

1.58
0.38
2.20
2.
84
0.99
0.58
0.
1.
0.
0.

2.
1.
0.
1.
1.
0.
1.
1.
0.
192.
63
55
78
00

10
24
47
27
00
79
27
45
83
92 65.74
201.07 65.31
176.
18 59.34
0.45
141.
.58 49.90
1.
1.
1 .
1.
1.
1.
1.
1.
1.

0.859-
0.
0.
0.
0.
0.
0.
0.
0.
0.
127.18 0.
135.76 1.
116.34 1.
1.
91.68 1.
020
024
026
032
037
038
042 123789-HxCDF
051
054

1.141
000
952
955
959
962
9" 3
976
983
992
997 13C12-HXCDF 478
000 13C12-HXCDF 678
017 13C12-HXCDF 234
034
.042 13C12-HXCDF 789




AN













SOR3
IS4
ALT2

ALT1
711.75
Uvr^^f / uiW"rsr*\ f ,-.! 1 Ai.tc-
05-1.43
1
1
1
2
0
1
2
1
4
0
2
10
0

.05
0
1
.08
.65
. 85
.54
.48
.70
.04
.84
.30
.77
.69
.08
.43

-1.43
.98
.79
0.97
0
.54
0.13
2
3
1
1
0
2
1
1
0
1
0
0
0
0

1
1
1

.29
.45
.52
.25
.70
.35
.21
.41
.99
.84
.72
.27
.96
.00

.75
.52
.68
0.79
0.42
0.950-1.015
0
0
0
0
0
0
0
0
0
0
1
1
1

0.966
0
0
0
. 000
. 957
. 964
. 9"'3
. 9~3
.980
.982
.991
.995
.998 123478-HxCDD
.001 123678-HxCDD
.009 123789-HxCDD
.018

-1.034
.000
.948
.954









AN
AN
AN






0.956
0.960
Triangle Laboratories, Inc.® Analytical Services Division
801 Capitola Drive • Durham, North Carolina 27713
Phone: (919) 544-5729 • Fax: (919) 544-5491
                                                                    Printed: 15:1909/18/1

-------
Page  No.     5
09/18/97

Conqpound/
M_Z.... QC.Log Omit Why
Listing of S975835B.db«
Matched GC Peaks /  Ratio / Ret. Time
.RT.  OK Ratio Total.Area... Area.Peak.1..  Area.Peak.2..  Rel.RT Compound.Name..  ID.. Flags.



402-404
HpCDF
408-410



403-410
13C 12 -HpCDF
413-420







418-420
HpCDD
424-426

D



424-426
13C12-HpCDD
436-438





436-438
DC WL 28:14 RO
DC SN 28:21 RO
DC SN 28:28 RO
DC SN 28:40 RO
DC SN 28:56 RO
DC SN 29:04 RO
29:13
29:18
29:35
DC SN 29:54
3 Peaks
0.
DC NL 0:00 RO
31:57 RO
DC SN 32:11 RO
32:24 RO
2 Peaks
0.
DC NL 0:00 RO
DC SN 31:05 RO
31:16
31:37 RO
DC SN 31:53
DC SN 31:59 RO
DC SN 32:07 RO
32:28
3 Peaks
0
DC NL 0:00 RO
DC SN 31:24 RO
DC SN 31:31
DC SN 31:52 RO
DC SN 32:00 RO
DC SN 32:18 RO
0 Peaks
0
DC NL 0:00 RO
DC SN 31:23
31:37 RO
32:07
32: 16 RO
DC SN 32:29 RO
3 Peaks
0.22
0.40
0.47
4.79
0.16
0.44
1.32
1.21
1.18
1.07

38-1.20
2.96
3.76
5.13
0.71

37-0.51
0.95
1 . 63
0.49
0.73
0.47
1.28
0.58
0.42

.88-1.20
0. 85
0.75
1.14
0.45
0.72
1.58

.88-1.20
1.77
0.94
1.30
1.03
0.57
5.68

1.01
0.85
1.01
0.96
0.33
0.42
127.00 72.36
144.74 79.14
293.62 158.87
2.54
565.36

2.24
2.53 4.66
0.61
5.00 2.55
7.53

2.12
1.77
83.95 27.59
2.85 1.44
1.74
1.66
1.24
54.54 16.23
141.34

1.79
1.41
9.13
1.33
1.65
1.96
0.00

1.75
0.64
3.26 2.08
71.73 36.31
2.47 1.26
0.75
77.46
0.964
0.968
0.972
0.978
0.987
0.992
54.64 0.997 13C12-HXCDD 478 SUR4
65.60 1.000 13C12-HXCDD 678 IS5
134.75 1.010 13C12-HXCDD 789 RS2
1.020

0.995-1.044
0.000
1.24 1.022
1.029
3.59 1.036

0.936-1.123
0. 300
0.994
56.36 1.000 13C12-HpCDF 678 IS6
1.98 1.011
1.020
1.023
1.027
38.31 1.038 13C12-HpCDF 789 SUR5 R

0.976-1.006
0.000
0.978
0.981
0.992
0.996
1.006

0.969-1.031
0.000
0.977
1.60 0.984
35.42 1.000 13C12-HpCDD 678 IS7
2.20 1.005
1.011

 Triangle Laboratories, Inc.® Analytical Services Division
 801 Caphola Drive • Durham, North Carolina 27713
 Phone: (919) 544-5729 • Fax: (919) 544-5491
                                                                   Printed: 15:19 09/tM
                                                                                                       199

-------
Page No.
09/13/97
Listing of S975835B.dbf
Hatched GC PeaXs / Ratio /  Ret. Tiro*
Compound/
M_Z.... QC.Log Omit Why ..RT.  OK Ratio Total .Area... Area. Peak. 1.. Area. Peak. 2. .  Rel.RT Conqsound. Name..  ID..  Flags.
OCDF
442-444
 442-444
0.76-
DC
DC
DC
DC
DC
DC
DC
DC
DC

DC
DC
DC
DC
DC

DC

NL
SN
SN
SN
SN
SN
SN
SN
SN

SN
SN
SN
SN
SN

SN
2
0:
31:
31:
32:
32:
32:
33:
33:
33:
33:
33:
34:
34
34
35
35
35
00
20
47
24
31
55
01
09
31
43
:54
:14
:45
:59
:07
:20
:51
RO
RO
RO
RO .

RO
RO

RO
RO
RO
RO
RO
RO
RO
RO
RO
0.
0.
0.
0.
0.
0.
1.
1.
1.
1.
0.
0
0
1
1
0
0
1.02
59
63
22
43
76
33
75
01
32
.74
,54
.46
.27
.76
.14
.61
.44
Peaks
                                             HpCDD / Octa-CDD and CDF Follows
                       1.17
                       2.02
                       0.47
                       2.00
                       0.90
                       1.19
                       1.30
                       1.39
                       1.70
                       2.95
                       2: 19
                       1.95
                       1.95
                       1.78
                       1.40
                       4.31
                       2.40
                       7.26
                                                              2.71
                                                              2.03
                0.884-1.116
                    0.000
                    0.903
                    0.916
                    0.934
                    0.937
                    0.949
                    0.951
                    0.955
                    0.966
                    0.972
                    0.977
                    0.987
                    1.001
                    1.008
                    1.012
                    1 .018
                    1.033
                                                                            1.56
                                                                            3.35
 OCDD                           0.76-1.02
 453-460         DC  NL   0:00      0.31
         AN              34:42      0.82
                         35:03  RO  0.63
 458-460               2 Peaks
                        1.52
                       60.40
                        3.38
                       63.78
27.20
 1.59
   0.384-1.116
       0.000
33.20  1.000 OCDD
 2.54  1.010
 13C12-OCDD                     0.76-1.02
 470-472         DC  NL   0:00 RO  1.89
                 DC  WL  34:24 RO  2.59
         M               34:42     0.80
 470-472               1 Peak
                        0.39
                        0.93
                       53 .40
                       53.40
23.80
                 0.995-1.005
                     0.000
                     0.991
              29.60  1.000 13C12-OCDD
                                           IS8  N
  Column Description	  "Why" Code Description	   Q_C  Log  Desc.
  M_Z    -Nominal Ion Mass(es)
  ..RT.  -Retention Time  (mm:ss)
  Rat.l  -Ratio  of M/M+2  Ions
  OK    -RO=Ratio Outside Limits
  Rel.RT-Relative Retention Time
      End of Report
         WL-Below  Retention Time Window
         WH-Above  Retention Time Window
         SN-Below  Signal  to Noise Level
         
-------
TiletS975835 #1-848 Acqtll-SXP-1997 13i40i51 XI* Voltage SIX 70S NoifetlSO
303.9016 T:2 BSUB(256,30,-3.0)  PKD(9,5,5,0.05\,720.0,1.00\,T,T) XxptEPCOS
TXIAHSLX LA3S  Text:I-H23-2    TLH43085
                      A4.
                                       A6.99E4
                                              A5.14X4
                                  A6.40E4
      17:00           18:00           15:00           20:00         ;  21:00
rilo:S975835 41-040 Acqill-SEP-1997 13:40»51 EH- Voltage SIX 70S Ot±ae:30
305.8987 T:2 BSUB(256,30*-3.0)  PKD(9,5,5,Q.05\,120.0,1.00\,r,T) XxptXPCUS
TRIANGLE LABS  Text:I-M23-2   TLH43085
1004                  A7.20E4
                                                                                      22100
      17:00           18:00           15:00           20:00           21:00
rile:S975835  41-848 Ac^:ll-srP-15S7 13:40:51 EH- Voltage SIX  70S No±ae:30
315.9419 T:2  BSUB(256,30,-3.0) PKD(9,5,5, 0. OS\,120.0,1. 00\,T, T) Exp-.EPCOS
TRIANGLE LABS  TextsI-M23-2   TLIf 43085
10 04                                                             A2.26E5

  80:

  50:

  40:

  20:
                                                                                      22': 00
       17:00           18:00           15:00           20:00           21:00
 file:S975835 41-848 Ac?:ll-srP-1597 13:40:51  EI+  Voltage SIX 70S Mtoi«e:33
 317.9389 T:2 BSUB(256,30,-3 .0) PKD( 9, 5,5, 0 . 05%,132. 0, 1. 00\,T, T) Exp:EPCUS
 TRIANGLE LABS  7ezt:J-K23-2   IXJ443085
                                                                 A2.92E6
   60:
   40:
   20:
                                                                                       22:00
       17:00           18:00           19:00           20:00
 rile.-S975835  41-848  Acg:ll-SEP-1997 13:40:51 EI+ Voltage SIX  70S
 330.9792 F:2  Exp:EPCDS
 TRIANGLE LABS  Text:I-H23-2   HJ443085

 IOOJ|  ..c.                           18:5919:19    jo.c,	
                                                                       21: 00
                                                                                       22:00
   8(9!

   60:

   40:

   20:

    0.
                                  V
        17:00           18:00           15:00           20:00
  rile:S575835 41-848 Acg:ll-srP-19S7 13:40:51  EH-  Voltage SIX 70S
  375.8364 T:2 ExptEPCUS
  TRIANGLE LABS  Text:I-M23-2   TLH43085
          17:09
                                                                       21:00
                                                                                       22:00
60:

40:

20:

 0.
                                                                        21:01
                                                                                             22:21
                                                                                          57.
                                                                                                    5.4X5

                                                                                                    4.315

                                                                                                    3 . 2ES

                                                                                                    2.1E5

                                                                                                    .1. 1E5

                                                                                                    .O.OEO
                                                                                                       Time



                                                                                                    .5.825

                                                                                                    .5. 5E5

                                                                                                    .4.ir5

                                                                                                    .2.7E5

                                                                                                    .1. 4E5
                                                                                                       O.OEO
                                                                                                           T±m
                                                                                                       3.OE6

                                                                                                       2.4E6

                                                                                                       1. 8E6

                                                                                                      -1.2E6

                                                                                                      .6.1E5
                                                                                                        O.OEO
                                                                                                           Tim
                                                                                                      -8.9E3

                                                                                                      '.7.1X3

                                                                                                      Ls.3X3

                                                                                                      1.3.6X3

                                                                                                       .1.8X3

                                                                                                        0.0X9
        17:00
                        18:00
                                        15:00
                                                        20:00
                                                                        21100
                                                                                        22100

-------
 'lieiSS75835 tl-848 Aeqill-SXP-1997  13i40i51 XI* Volt*7* SIX 70S Hoim»t29
 '19.8965 Tt2 BSOB(256,30, -3.0)  PB>(7,5,3, 0.05\, 116.0,1.00\,r,T) KiptXPCVS
TRIANGLE LABS  Tejct: I-M23-2   TLH43085
100.1
                   15:00               20:00               21:00
rilatS975835 #1-848 Aoqill-SXP-1997 13:40:51 EH- Voltage SIS 70S Koite:34
321.8936 r>2 BSUB(256,30,-3.0)  PKD(7,5,3,0.05\,136.0,1.00\,f,T) XxpiXPCUS
TRIANGLE LABS   Text:I-H23-2   TLH43085
1001
                                                   A4  52E3     A1.16E4 A9.59E3
                                                        A1.12E4
                                                                              22:00
                    19:00              20:00               21:00
rile:S975835  #1-848 Acq:ll-SEP-1997 13:40:51 EI+ Voltage  SIS  70S Noiae:925
331.9368 r-.2  BSUB(256,30,-3.0) PKD(7,5,3,0.05\,3700.0,1.00\,r,T) Exp:EPCOS
TRIANGLE LABS  Text: J-M23-2   TLH43085
1001
                                                                              22:00
  801

  601

  401

  201

   Ol
                               \A2.09E6
                    19:00              20:00               21:00
 rile:S975835 #1-848 Acq:ll-SEP-1997 13:40:51 XI+ Voltage SIR 70S Noise:37
 333.9338 T:2 BSUB(256r 30,-3 .0) PKD( 7, 5, 3, 0. 05\,148. 0,1. 00\,f, T)  Exp:EPCUS
 TRIANGLE LABS  TextiI-M23-2   TLI#43085
                                          22:00
 1001

  aoi

  601

  401

  201

   0.
                           A4.74E6
                               A2.59E6
                    19:00               20:00              21:00
 r±le:S97583S #1-848 Acq:ll-SEP-1997 13:40:51  EI+ Voltage SIS 70S Noise:26
 327.8847 T:2 BSUB(256,30, -3. 0) PKD(7,5,3, 0.05\,104. 0,1. 00*,T,T) ExpsEPCUS
 TRIANGLE LABS  TextiI-H23-2   TLI#430B5
 100*                                                               A4.03E6

  801

  601

  401

  201

   01
                                          22: 00
Al.09E6
                      T
                   19:00               20:00               21:00
rile:S975835 #1-848 Acq:ll-SEP-1997 13:40:51 EI+ Voltage SIS 70S
330.9792 F:2 ExptEPCUS
TRIANGLE LABS  TeztiI-H23-2    TLH43085
1001
                   18:59  19:19      19,52
 8
-------
  .le,S975835 tl-848 Aoqill-SXP-1997 13,40,51 XX+ Voltage SIX  70S Nolfe,35
 39.8597 r,2 BSDB(256,30,-3.0)  PXD(7,5,3,0.05\,140.0,1.00\,T,T) XxpiXTCOS
TXIAMGLX LABS  Text,I-M23-2   TLH43085
  OOS

  sol
 40.

 20:

  0.
              23100                 24,00                 75*00
 ile,S975835 tl-848 Aoqill-SXP-1997 13,40,51 EI+ Voltage SIX 70S Nolle,216
 41.8567 F,2 BSUS(256,30,-3.0)  PKD(7,5,3,0.OS\,864.0,1.00\,r,T) XxptXPCOS
TRIANGLE LABS  Text,I-H23-2  TLH43085
 004       Al.  5X5
               23,00                24i00                25,00
 ile,S975835 tl-848 Acqsll-SEP-1997 13,40:51 EI+  Voltage  SIX 70S Noiae,31
 51.9000 T:2 BSOB(256,30,-3.0) PKD(7,5,3,0.05\,124.0,1.00\,T,T) ExptEPCVS
 TRIANGLE LABS  Tejct,I-H23-2   TLH43085
  00\                                                 A2.16E6
                                                                      Al.77E6
A*.

» 	 J
I3f3
AS. 01X4


\AS.27X3 IA6.96X3 / \ *! *i A9 . a 3Z3 *1 •* **£
\«* _*p«A-A n ..A .A / ™ - yJlvsJ'^yAA/^ -A» A AV1ilL>/\ As


AS. 08X4
^Ar




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I A * N19.99X3
nJU^t* I\*A./\ At JA.
                                                                              26,00
                                                                                                     5.1X4

                                                                                                     4.1X4

                                                                                                     3.1X4

                                                                                                     2.0X4

                                                                                                     1.0X1

                                                                                                     0.0X0
                                                                                                         TiM*
                                                                             26,00
               23,00                24,00                 25:00
 rilesS975835 91-848 Acq:ll-SEP-1997  13,40,51  EH- Voltage SIX 70S Jtoiaes37
 353.8970 Fs2 BSUB(256,30,-3.0)  PKD(7,5,3,0.051,148.0,1.00\,F,T) ExpiEPCUS
 TRIANGLE LABS  TextsI-M23-2    TLIf43085
 100*                                                  ,, ,OM        A1.24E6
                                                                               26,00
  60:

  40:

  20.

   0.
                                                       A1.39E6
                                                       4
                                                                                                      6.4X5

                                                                                                      5.1E5

                                                                                                      3.8E5

                                                                                                      2.6E5

                                                                                                      .1. 3X5

                                                                                                      .O.OEO
                                                                                                         Tim.



                                                                                                      .4.1X5

                                                                                                      .3. 3E5

                                                                                                      .2.5X5

                                                                                                      .1. 7E5

                                                                                                      .8.3X4
               23,00                 24,00                25', 00
rile,S97S835 fl-848 Acqsll-SEP-1997 13,40,51 EI+ Voltage SIX  70S
330.9792 T:2 XxpiEPCOS
TRIANGLE LABS   Text,I-M23-2   TLH43085
                                                                               26,00
                                                                                                       O.OEO
                                                                                                          Tim
               23,00                24', 00                25:00
rile:S975835 tl-848 Acqtll-SXP-1997 13,40,51 EH- Voltage  SIX 70S
409.7974  T:2 ElpiEPCDS
TRIANGLE LABS  TextsI-M23-2   TLH43085
                                                                               26,00
                23,00
                                     24,00
                                                          25100
                                                                               26,00
                                                                                                           20

-------
 '±1.,SS75B3!, U-B4B Acq,11-3X9-1997 13,40,51 tit Voltage 3TI 70S Hoite:33
355.8546 fi2 BSOB(256, 30, -3.0) HO>( 7,5, 3, 0.05%, 132.0,1.00\,T,T)  KlptfPCUS
TXIAJKUS LABS' TeJCttI-M23-2   TLH43085
        24100                          25'tOO                         26100
rilei3975835 41-848 Acqtll-SXP-1997 13i40i51 EI+ Voltage SIX 70S Wo±»e,35
357.8516 Tt2 BSU3(356,30,-3.0) PKD(7,5,3,0.05\t140.0r1.00\,T,T) ElpiIPCOS
TRIANGLE LABS   T»xttI-M23-2   TLH43085
IOC
        34:00                          25:00                         26', 00
Tile:S975835 H-848 Acqill-SEP-1997 13:40:51 EI+ Voltage  SIR 70S Xoiaes31
367.8949 T:2 BSVB(256,30, -3. 0) PKD(7,5,3, 0. 05\,124. 0,1.00%,T, T)  Eip:EPCUS
TRIANGLE LABS  TeitsI-M23-2   TLI«43085
                                                                     A1.14E6

 80.

 60:

 40.

 20:

   0.
         24:00                         25:00                         26:00
Tile:S97583S tl-848 Acqsll-SEP-1997  13:40:51 EI+ Voltage SIX 70S Noime:26
369.8919 T:2 BSU3(2S6,30,-3.0) PKD(7,5,3,0.05\,104.0,1.00\,F,T) Elp:EPCUS
TRIANGLE LABS  Tejct:I-M23-2   TLI#43085
                                                                     A8.J.2E5

  80.

  60.

  40.
  20.

   0.
         24:00                         25:00
 FiletS97583S il-848 Acq:ll-SEP-1997 13:40:51 EI+ Voltage SIX  70S
 330.9792 Tt2 ExptEPCUS
 TRIANGLE LABS  Text:I-M23-2    TLH43085
                                                                     26*: 00
                                                                           . 06E5
                                                                           A
                                                                                                  0.0X0
                                                                                                     Tim»\
                                                                                                  O.OEO
                                                                                                      T±me
3.3E5

2.6E5

2.0E5

1. 3E5

6.6E4

O.OEO
   Time



.2.4E5

1.9E5

.1.4X5

.9. 7E4

.4.8E4

.O.OEO
   Tim.
                                                                                                              20

-------
Tilm:S97583S #1-405 Acq:ll-BXf-1997 13i40i5l  XI +  Voltage SIX 70S Noime:689
373.8208 Tt3 *SUS(256,30,-3.0) HO)(7,5,3,0.05\,2756.0,1.00\rr,T) XzptXPCPS
TXIAHSLX LASS  Text:I-H23-2   TLH43085
1001                          A2. 1X4
                                                                                                        5X3

                                                                                                        0X0
         27i24~  37. «7»8« 00fl   aafl    2flsJ5' 28t48' 29\00  29'>i2' 29\24' 29i36' 29t48 3b',00' 3»tl2    Time
rile:S975835 il-406 Acqill-SSf-1997 13i40t51 EI+ Voltage SIX 70S Boi*»:633
375.8178 r:3 BSUS(256,30,-f.O)  rXD(7,5t3,O.OS\,2532.0,1.00\rTrT) Xlp:EPCUS
TXIAVSLX LASS   Text:I-M23-2   TLII43085
                A2.89E4
   27:12 37,24 27:36 27:48  28:00 28:12 28>24 28:36  28:48 29:00 29:12 29:24  29:36 29:48 30:00  30:12
 r±letS975835 il-406 Ac
-------
 'iJ.«lSS758J5 *1-4QO Aoqill-SXf-1997 1J,40:51 XI* VoltMge SIX 70S
 89.8156 Tt3 BSOB(256,30, -3.0)  PO>(7,5,3,0.05\,2388.0,1.00\,T,T) XxptKPCOS
TRIANGLE LABS  T*j[t,I-M23-2   TLH43085
100*                                                        A1.89E4
    27,48    28:00   28,12   28:24    28:36   28:48   29,00    29,12   29,24
Tile,3975835 tl-406 Acq:ll-SXP-1997 13:40:51 EI+ Voltage SIS 70S NoitetSSO
391.8127 T:3 BSUB(2S6,30, -3. 0)  PJO>(7,5,3, 0.05\,2200. 0,1. 00\,T,T) EzpiEPCVS
TRIANGLE LABS  Text,I-H23-2   TLIt43085
 80.

 60.

 40.

 20.
A3.54X4
                                                                         A1.36E4
                                                                               29,36    29,48
                                                                                          .23X4
   0.
    '27:48   28:00   28:12    28,24   28:36   28:48    29:00    29:12   29:24
rile:S97S835  tl-406 Acqsll-SEP-1997 13,40,51 EI+ Voltage SIR  70S Nbiae:478
401.8558  r,3  BSUB(256,30,-3.0) PKD( 7,5, 3, 0.05\,1912. 0,1. 00%, T,T) Exp:EPCUS
TRIANGLE  LABS  Teit:I-M23-2   TLIt43085
1004
  so;
  so;

  40.

  20.
                                                                   29:36   29:48
                                                                              Al.59E6
                                                     A7.91E5
     27:48   28:00   28:12    28:24   28:36   28,48    29:00   29:12   29:24
File:S975835  tl-406 Aoq:ll-SEP-1997 13:40:51 EH- Voltage SIR  70S Noite:490
403.8529  T:3  BSUB(256,30,-3.0) PXD(7,5,3,0.05\,1960.0,1.00\,T,T) ExpiEPCUS
TRIANGLE  LABS  Text:I-H23-2   TLH430S5
1001
  ao:
  so:

  40.

  20:
                                                                                29:36   29:48
                                                                              A1.35E6
                                                     A6.56E5
     37148   28:00    38:13   28:24   28:36  ' '28\4829\66   29:12
 Tile:S975835 tl-406 Acq:ll-SEP-1997 13:40:51 EI+  Voltage SIR 70S
 392.9760 T:3 Xxp:XPCUS
                Text:I-M23-2   TLIt43085
                                                                        29:24
                                                                                 i i  i *n 'i i' i i *i
                                                                                29:36   29:48
                        38:16
TRIANGLE LABS
100^
    27:48    28:01
 BO:

 601

 40.

 20:

  o:
                                  28:30
                                             28:45
                                                     28:56.
                                                           9:04
                                                                    29:19  29:29
                                                                                                .1.4X4

                                                                                                .1.1X4

                                                                                                .8.5X3

                                                                                                .5.6X3

                                                                                                .2.8X3
                                                                                    ,0.0X0
                                                                                        T±m«
                                                                                                .6.8X3

                                                                                                _5.4E3

                                                                                                .4.1E3

                                                                                                .2.7X3

                                                                                                .1. 4E3

                                                                                                  O.OEO
                                                                                                     Time



                                                                                                _5. 8E5

                                                                                                '.4.6X5

                                                                                                -3.5E5

                                                                                                -2.3E5

                                                                                                 .1.2E5
                                                                                     O.OEO
                                                                                        Time
                                                                                                 .4.6X5

                                                                                                 '.3. 7X5

                                                                                                 -2.8X5

                                                                                                 .1.9X5

                                                                                                 .9.3X4
                                                                                     0.0X0
                                                                                        Tim
                                                                                          29:50
                                                                                    .2.1X6

                                                                                    11.7X6

                                                                                    '.1.3X6

                                                                                     .8.6X5

                                                                                     .4.3X5
     27:48   28,00    28,12   28,24    28,36   28,48
                                                       29:00
                                                   29\12
                                                                       i  i I i  i i  i i I  i i i  i i  I i i
                                                                       29:24   29:36   29,48
                                                                                                 .0.0X0
                                                                                                    Time
                                                                                                       206

-------
 ±l»tS97S835 fl-430 Acqill-SEP-1997 13:40,51  11+ VoJLtag* SIX 70S Nolle:1628
 07.7818 T>4 B8UB(356,30,-3.0) tKD(7,5,3,0.05\,6513.0,1.00\,T,T) XxpiXPCUS
TRIANGLE LABS  TmxtiI-M23-2   TLH43085
                             A3.57X4
           31tl3      31,24      31': 36     3l'i48     32': 00     32:12     32:24
 iletS975B35 tl-430 Acqtll-SEP-1997 13:40:51 EI+ Voltage SIS 70S No±*e:548
 09.7789 ri4 BSUB(256,30,-3.0)  PKD(7,5,3,0.051,2192.0,1.00%,T,T) XxptXPCOS
TRIANGLE LABS   TexttI-H33-3   TLH43085
 001
           31:12      31:34     31:36     31:48      33:00     33:12      33:34
F±le:S975835  fl-430 Acq:ll-SEP-1997 13:40:51 EI+ Voltage SIR  70S Noiie:697
 17.8353 T:4  BSUB(356,30, -3. 0) PKD(7,5,3, 0. 05\,3788. 0,1. 00\,T, T) ExpiEPCOS
TRIANGLE LABS  Text:I-M33-3   TLH43085
  001          A2. 76E5
                                                                                   32:36
                                                                                              32:48
           31:12     31:24      31:36     31:48     32:00      32:12     32:24
r±le:S97SS35 fl-430 Acg:ll-SEP-1997  13:40:51 EI+ Voltage SIR 70S Noise:733
419.8220 T:4 BSUB(256,30,-3.0)  PKD(7,5, 3, 0. 05\,2932. 0,1. 00\,T, T) Exp:EPCUS
TRIANGLE LABS  Text:I-M33-2   TLH43085
1001         A5.64E5
                                                                                    32:36
  so:
  60.
  40:
  30:
   o.
                                                                            A3.83E5
                                    Al.64E4
                                                                   A2.01E4
             T
                                  ~r
                                                       rr
                                                                T
            31:12     31:24      31:36     31:48     32:00      33:13
 rile:S975835 fl-430 Acq:ll-SEP-1997  13:40:51  EI+ Voltage SIR 70S
 430.9739 T:4 Exp:EPCUS
 TRIANGLE LABS  Text:I-M23-2   TLI#43085
                                                                         32:24
   TY^P i  i^r-i |"7 .
   32:36     32:48
 1003

  80:

  50:

  40:

  20:

   o:
          31:11
                31:17
                                31:36
                                               31:54   33:03
                                                                             33:39
                                                                                      33:38
                                                                                              33:48
              T
                        T
                                  "T
                                             ~T
            31tl3      31:34      31:36     3l':48      33'tOO      33:13
 rile:S975835 fl-430 Acq:ll-SEP-1997 13:40:51 EI+ Voltage SIR 70S
 479.7165 F:4 ExpsEPCUS
 TRIANGLE LABS   Tejct:I-H33-3   TLIf43085
                                                                          33\24
i  i i  i  i  i t  i  i  I i
   32:36     33:48
                    .O.OEO
                        Time
.1. 3E5

.1. OE5

.7.8E4

.5.3E4

.2.6E4

.O.OEO
    Tim<



.3.0E6

.1. 6E6

.1.2X6

.7.9E5

 3.9E5
 O.OEO
    T±m
 1001
                                  31:37
            31:12
                       31:24
                                 31:36
                                            31:48
                                                      32:00
                                                                32:12
                                                                          32:24
                                                                                     32:36
                                                                                               32:48

-------
 ld.eiSH7SSJS fl-430 Aoqill-SXr-1997 Ml40151 XI+ VoJitMg* SIX 70S aoi*mi437
 \33.7766 Tt4 BSUB(256,30, -3.0)  PXD(7,5,3,0.05\, 1828.0,1.00\,T,T) Exp:XPCUS
TRIANGLE LABS  T*xt:I-H23-2    TLH43085
100*
    31>1S  31': 24   31:30  31:36  31i42  31': 4 8  31:54   32:00   32:06  32tl2  32:18
riletS975835  #1-430 Acqtll-SXP-1997 13:40:51 XX+ Voltage SIX  70S Noise:536
425.7737 T:4  BSVB(2S6,30, -3.0) PKD(7,5,3,0.05\,2144.0,1.00\,r,T) XxpiXPCOS
TRIANGLE LABS  TexttI-M23-2   TLH43085
1001              A4.27E4
                                                                                   32124
                                                                                          32^30
  80.
  60.
  40.
  20.
                                                              A2.93X4
                    ~T
                           ~T
                                                 T
                                                        T
    31:18   31:24  31:30  3l':36  31:42  31:48   31:54   32\00  32:06  32:12  32:18
rile:S975835 tl-430 Acqtll-SEP-1997 13:40:51 XI+ Voltage  SIX 70S KOitet759
435.8169 f:4 BSW3(256, 30, -3. 0) PXD(7,5, 3, 0. OS\, 3036. 0,1. 00\,T,T) Eip-.EPCOS
TRIANGLE LABS  Text:I-M23-2   TLH43085
1003,                                                           A3.63E5

  so:

  60:

  40.
                                                                                   32:24  32:30
  20.
                          A2.08E4
                                     Al.39E4
                                                                                         A2.10E4




    31:18  31:24  Jl   O   31  36  3142  31  s   154  32     32: 06  32:12
r±le:S975835 #1-430 Acq:ll-SEP-1997 13:40:51 XI+ Voltage SIX 70S Noise: 428
437.8140 r:4 BSUS(256 , 30, -3 .0 ) PKD( 7, 5, 3, 0 . 05\,1 712. 0,1 . 00\,T, T) Eip:EPCVS
TXIANGLE LABS  Text:I-M23-2    TLI#43085
                                                                                           3^30
 1001
  801
  60.
  40:
  20.
                                                                A3.S4E5
                           Al.60E4
                                          A2.81X4
                                   T
                                          T
~r
     31:18  31t24  31,30  31:36   31:42  31:48  3l't54  32:00  32:06
 r±le:S975835 H-430 Acq:ll-SEP-1997 13:40:51 EI+ Voltage SIX 70S
 430.9729 F:4 ExpsXPCUS
 TXIANSLE LABS  Toxt:I-M23-2   TLI#43085
                                                                           A2.20E4
                                                                                         Al. 64E4
                                        .0.0X0
                                            T]JU
                                         1. OE4

                                         8.2X3

                                         6.2X3

                                         .4.1X3

                                         .2.1X3

                                         .O.OEO
                                            Tixe



                                         .8.3X4

                                         .6.6X4

                                         .5.0E4

                                         .3.3E4

                                         .1. 7X4

                                         .O.OEO
                                            Time



                                         .8.1E4

                                         .6.5X4

                                         .4.9X4

                                         .3.3X4

                                         .1. 6X4
                                                                            32:18  32:24  32:30
1003

  80.

  601

  40.

  20.

  0.
                   31:29  31:36
                                                           32:03
     31:18  31:24  31:30
                                           '
                                 3142  3l,48   3154
                                                                     33:13
                                                                                    '32\24
0.0X0
   Time
                                         1.9E6

                                         1.5X6

                                         1.2X6

                                         7.7X5

                                         3. 9X5

                                         0.0X0
                                             Time
                                                                                                        208

-------
    Al. 73X4
F11*:S975835 tl-430 Acqill-SXP-1997 13i40i51 11+ Voltage SIX  70S Koif»:276
441.7428 f:4 BSUB(256,30,-3.0)  PXD(7,5r3,0.05\,1104.0,1.00\,r,I) XxftXfCOS
TXIANGLE LASS  Tmjct: I-H23-2   TLH43085
1003
 901
 80.
 701
 601
 50J
 40.
 30.
 20.
 10.
   0.
          3l':00	32:00            33:00             34:00
rila:S975835 #1-430 Aoq:ll-SXP-1997 13:40>51  XH- Voltage SIX 70S Hoif»,464
443.7399  T-.4 BSUB(256,30, -3. 0) PKD(7,5,3, O.OS\,18S6. 0,1.00\,T, T) ExptEPCUS
TRIANGLE  LASS  TextsI-M23-2   TLH4308S
1003k            A2.  7E4
                                                                                     A2.03E4
                  Al.76X4
          A2.46E4
                              A1.22E4
    A1.50E4  A2.71C4
A1.21X4\
                                                          2.4X4
                                                          .2.2X4
                                                          .1.9*4
                                                          a. 7X4
                                                          .1.4X4
                                                          JL.2X4
                                                                                35:00
         31': 00             32:00             33:00             34:00
F±le:S975B35 #1-430 Acq:ll-SEP-1997 13:40:51 EH- Voltage SIX  70S
430.9729 r:4 Exp:EPCUS
TSI ANGLE LABS   Text: I-M23-2   TLHH3085
lOOi
          31:00             32:00             33:00             34:00
 f±le:S975835 91-430 Acqtll-SEP-1997 13:40:51 EH- Voltage SIS 70S
 513.6775 T:4 Exp:EPCUS
 TRIANGLE LABS  T&xt:I-M33-2    TLIH3085
 1001
  801
  70.
  60.
  501
  40.
  301

  10.
                                                   33:18
                                                            33:'.
                                                                   34:11
                                                                         34:30
                                                                                  35:00
                                                                                  35:01
                                                                                 35:00
                                                                                                        2.1E6
                                                                                                        1. 9E6
                                                                                                        1. 7E6
                                                                                                        1.5E6
                                                                                                        .1.2E6
                                                                                                        .1. 0X6
                                                                                                        .8.3E5
                                                                                                        .6.2E5
                                                                                                        .4.1ES
                                                                                                        .2.1X5
                                                                                                       .0.0X0
                                                                                                          Tim
                                                                                                           20

-------
 'U»:S975B35 H-130 \oytll-3Sf-1997 MtiOiSl K+ Voltage S» 70S lbim»,342
 57.7377 ri4 BSDB(256, 30,-3.0)  PKD(7,5,3,0.05\,1368.0,1.00\,r,T) XxptXTCOS
TXIAHGLE LABS  T*xttI-M23-2   TLIH308S
 001                                        A2.84E5
 80.

 60.

 40.

 201
       34,24         34:30         34:36         34:42         34,48         34:54
 ile:S975835  $1-430 Acqill-SXP-1997 13:40,51 XI+ Voltage  SIX  70S «Oi»»:418
 59.7348 F:4  BSOB(256,30, -3. 0) PB>(7,5,3, 0. 05%, 1672. 0,1. 00%,T, T) Xxp:XPCVS
TRIANGLE LABS  T»It:I-M23-2   TLH43Q85
10 0\                                                A3. $1X5
  80.
  60.
  40.
A2.20X4
                                                                                          35100
.3.0X4

'.2.4X4

11. 8X4

.1.2X4

.6.0X3
                                                                                                  0.0X0
                                                                                                     Tim,
  201
                   A7.55E3
                                                                                            3.9X4

                                                                                           .3.1X4

                                                                                           .2.3X4

                                                                                           LI. 6E4

                                                                                           .7.8E3
       34:24         34:30         34:36        34:42         34:48         34:54
 rile:S975835 #1-430 Acqtll-SEP-1997  13:40:51  EH- Voltage SIX 70S Soite:443
 469.7779 F:4 BSOS(256, 30, -3. 0) PKD( 7,5,3, 0. 05\,1772. 0,1. 00\,T,T) Eip:EPCUS
 TRIANGLE LABS  T*xtiI-H23-2   TLH43085
 1001                                           A1.73E5
                                                                                                  0.0X0
                                                                                          35:00      Tim,
       34:24         34:30         34:36         34:42         34:48         34,54
 rile:S975835 H-430 Acq:ll-SEP-1997 13:40:51 XI+ Voltage SIX 70S  Hoiae:235
 471.7750 r,4 BSUB(256,30,-3.0)  PKD(7,5,3, 0. 05\,940. 0,1. 00%,T, T) Sxp:EPCUS
 TRIANGLE LABS  Text.:I-M23-2   TLH43085
 1001                                            A2.98E5
  80.
   60.
   40.
                                                                                           35,00
   201
         A4.B7E3
                                                                                             3.5E4

                                                                                            .2.8X4

                                                                                            .2.1X4

                                                                                            .1.4E4

                                                                                            .7.0E3
        34:24         34:30         34:36         34:42         34:48
 r±le:S975835  H-430 Acq:ll-SEP-1997 13:40:51 EH- Voltage SIX 70S
 430.9729 Ti4  ExpiEfCUS
 TRIANGLE LABS  Text:I-H23-2   TLU430B5
  1003

   80.

   60.

   40.

   20.

    0.
                     34:30
                                         34:41
                                                  34:45
                                                                             •34:54
                                                                       34154
                                                                                           35:00
                                                                                             .0. OSO
                                                                                                Tim
 -2.1E6

 -1. 7X6

 .1.2X6

 -.8.3X5

  .4.1X5
        34:24
                      34130
                                    34:36
                                                  34:42
                                                               34:48
                                                                             34:54
                                                                                           35:00
                                                                                              0.0X0
                                                                                                 Tim

-------
              -430 Acq:ll-SEP-i997 II:
EI+ Voltage SIR
                               File Text:I-M23-2   TLI#43085
                                              32:28
           3i:00                    32;00                   33:00
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                               File Text:I-M23-2   TLI#43085
                                               32.29
                                                                                           Time

-------
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23.7766 F:4 Exp:EPCUS
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          31:00                    32:00                    33:00
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25.7737 F:4 Exp:EPCUS
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          31:00                   32:00                    33:00
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35.8169 F:4 Exp:EPCUS
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-------
TLI Project:      43085
Client Sample:   I-M23-3
Method 23 PCDD/PCDF Analysis (a)
             Analysis File:   S975843
Client Project:
Sample Matrix:
TLI ID:

Sample Size:
Dry Weight:
GC Column:
S413-004
M23Train
181-55-7ABD

1.000
n/a
DB-5

Date Received:
Date Extracted:
Date Analyzed:
Dilution Factor:
Blank File:
Analyst:

09/03/97
09/04/97
09/11/97
n/a
S975815
KB

Spike File:
ICal:
ConCal:
% Moisture:
% Lipid:
% Solids:

SPX23704
SF56117
S975839
n/a
n/a
n/a
Analytes
2,3,7,8-TCDD
1,2,3,7,8-PeCDD
1,2,3,4,7,8-HxCDD
1,2,3,6,7,8-HxCDD
1,2,3,7,8,9-HxCDD
1,2,3,4,6,7,8-HpCDD
1,2,3,4,6,7,8,9-OCDD
2,3,7,8-TCDF
1,2,3,7,8-PeCDF
2,3,4,7,8-PeCDF
1,2,3,4,7,8-HxCDF
1,2,3,6,7,8-HxCDF
2,3,4,6,7,8-HxCDF
1,2,3,7,8,9-HxCDF
1,2,3,4,6,7,8-HpCDF
1,2,3,4,7,8,9-HpCDF
1,2,3,4,6,7,8,9-OCDF
totate
Total TCDD
Total PeCDD
Total HxCDD
Total HpCDD
Total TCDF
Total PeCDF
Total HxCDF
Total HpCDF
Amt. (ng)
ND
ND
ND
ND
ND
0.14
16.2
0.01
ND
ND
0.02
ND
EMPC
ND
0.04
ND
ND
Amt (ng)
ND
ND
0.02
0.34
0.01
EMPC
0.03
0.04
BL £WPC
0.005
0.009
001
\Jt\J i.
0.01
0.01



0.005
0.005

0.006
0.006
0.008

0.02
0.05
Number Dt SMPC
0.005
0.009
1 0.05
2
1 0.02
0.01
2 0.05
1
ftalfo «T ~ Flags



	

1.07 32:09 B~
0.87 34:39 	
0.70 20:26 B_


1.21 28:22

	

1.02 31:15 iZ

	
flags



.._


SL
-^^
                                        Page 1 of 2
                                                                          X237JPSR vlOO. LARS 6.10.&
Triangle Laboratories, Inc.®
801 Caprtola Drive • Durham, North Carolina 27713
Phone: (919) 544-5729 • Fax: (919) 544-5491
                       Printed: 15:19 09/18/91
                                    21

-------
TLI Project:      43085
Client Sample:   I-M23-3
Method 23 PCDD/PCDF Analysis (a)
             Analysis File:   S975843
Internal Standards
13Cl2-2,3,7,8-TCDF
13C,2-2,3,7,8-TCDD
13C,2-l,2,3,7,8-PeCDF
'3C,2-l,2,3,7,8-PeCDD
'3Ci2-l,2,3,6,7,8-HxCDF
13C,2-l,2,3,6,7,8-HxCDD
13C,2-l,2,3,4,6,7,8-HpCDF
13C,2-l,2,3,4,6,7,8-HpCDD
I3C12-1,2,3,4,6,7,8.9-OCDD

Surrogate Standards (Type A)
37CL,-2,3,7,8-TCDD
13C,2-2,3,4,7,8-PeCDF
13C,:-l,2,3,4,7,8-HxCDF
13Cr-l,2,3,4,7,8-HxCDD
13Cr-l,2,3,4,7,8,9-HpCDF

Alternate Standards (Type A}
13Ci2-l,2,3,7,8,9-HxCDF
13C,2-2,3,4,6,7,8-HxCDF
:::Re«»ro#Stand»^^^
13CI2-1,2,3,4-TCDD
13C,2-l,2,3,7,8,9-HxCDD
Amt« (ng) -,
2.5
2.3
2.3
2.3
2.6
2.3
1.4
1.2
1 3

; Amt, (ng)
4.1
3.7
4.5
40
30

Amt (rig)
2.2
2.9
!^'.

-.. % Recovery
*• f f •*
63.3
58.5
56.9
57.2
645
580
35.3
29.8
160

% Recovery:
103
93.4
112
99 8
75 7

% Recovery
54.2
73.5


QC Limits
40%-130%
40%-130%
40%-130%
40%-130%
40%- 130%
40%- 130%
25%-l30%
25%-130%
25%- 130%

QC Limits
70%- 140%
70%- 140%
70%- 140%
70%- 140%
70%- 140%

-QC Limits
40%-130%
40%- 130%


, Ratio
f
0.76
0.80
1.50
1.55
049
1 14
0.42
1.03
088

Ratio .
1.49
0.45
1 31
0 39

.•:'.;:;:;:':::-Ratio
0.48
0.48
Ratio
0.80
1.22
IflF / Ftegst,? -
20:24 	
21:13 	
24:42 	
25:50 	
28'29 Q
•79-12
31:14 	
32:07 	

RT Flags
21:14 	
25:28
28:22 	
-59.97

RTvr.iflagsv;
29:44 	
28:59 	
RT Flags
21:00 	
29:31 	
                      Data Reviewer.
                                         Page 2 of2
             09/18/97
                                                                          X237.PSR »2.00. LARS 6.1OM
 Triangle Laboratories, Inc.®
 801 Caprtola Drive • Durham, North Carolina 27713
 phone: (919) 544-5729 • Fax: (919) 544-5491
                       Printed: 15:19 09/18/97
                                   21*

-------
Data Review By:
                       Initial   	Date...

                         *yV~     I  / /8/  iT Calculated Noise Area:
                                                                      1.87
The Total Area  for each peak with an ion abundance  ratio outside
ratio limits  has been recalculated according to method requirements.
Page No.
09/18/97
Listing of S975843B.dbf
Matched GC Peaks  /  Ratio  / Ret. Time
Compound/
M_Z.... QC.Log Omit Why  ..RT. OK Ratio Total.Area...  Area.Peak.1.. Area.Peak.2..  Rel.RT Compound.Name..  ID.. Flags.

                                                                            0.818-1.101
                                                                                0.000
                                                                                0.852
                                                                                0.879
                                                                                0.924
                                                                                0.967
                                                            5.33          9.07  0.977
                                                                                0.991
                                                            7.65         11.00  1.002 2378-TCDF       AN
                                                                                1.062
                                                                                1.094
                                                                                1.110
TCDF
304-306 DC
D DC
D DC
DC
DC

DC
M
DC
D DC
DC
304-306

NL
SN
5N
SN
SN

SN

SN
SN
WH
2

0:
17:
17:
18:
19:
19:
20:
20:
21:
22:
22:

00
23
56
51
44
56
13
26
40
19
39
0.
RO
RO
RO
RO
RO
RO
RO




65-0.89
0.
45.
57.
0.
0.
0.
1.
0
0
0
0
21
05
19
29
.24
.59
.94
.70
.69
.85
.71
Peaks
0.
5.
5.
3.
1.
12.
2.
18.
2
9
3
30
83
27
12
40
.59
.25
.80
.65
.76
.84
.82
.90
 13C12-TCDF
 316-318
 316-318

DC
DC


DC
DC
DC


NL
WL


SN
WH
WH
2

0:
19:
19:
20:
20:
21
22

00
12
55
24
40
:36
:29
0.

RO
RO

RO
RO
RO
65-0.89
0.
1.
0.
0
0
0
0
,79
45
.91
.76
.10
.02
.32
Peaks
1.
4.
14.
4,035
4
6
8
4,050
97
,90
.76
.54
.44
.67
.14
.30
                                                    0.951-1.049
                                                        0.000
                                                        0.941
                                     7.55          8.34  0.976
                                 1,747.71      2,287.33  1.000 13C12-2378-TCDF ISO
                                                        1.013
                                                        1.059
                                                        1.102
                                       Above:  TCDF /  TCDD Follows
 TCDD
 320-322
  320-322
0.65-0.89
DC
DC
DC
DC
DC
DC
DC
DC
DC
DC
DC
DC
DC

NL
SN
SN
SN
SN
SN
SN
SN
SN
SN
SN
SN
WH
0
0:
18:
18:
18:
18
19
19
20
20
21
21
22
22
00
12
:21
:36
:48
:10
:30
:24
:49
:04
:22
:04
:33
RO
RO
RO

RO
RO
RO
RO
RO
RO

RO
RO
0.
0.
0.
0.
1.
3.
2.
3
0
0
0
0
2
61
95
32
70
,08
.87
.72
.10
.63
.52
.69
.45
.09
Peaks
                                                0.85
                                                2.99
                                                2.74
                                                1.65
                                                4.99
                                                1.10
                                                0.83
                                                4.96
                                                0.39
                                                2.80
                                                1.45
                                                0.92
                                                1.13
                                                0.00
                                                     0.851-1.058
                                                        0.000
                                                        O.S58
                                                        0.865
                                                        0.877
                                                        0.886
                                                        0.903
                                                        0.919
                                                        0.962
                                                        0.981
                                                        0.993
                                                         1.007
                                                         1.040
                                                         1.063
  37C1-TCDD
  328
                 DC  NL   0:00
                                                 0.28
                                                     0.906-1.094
                                                         0.000
 Triangle Laboratories, Inc.® Analytical Services Division
 801 Capitola Drive • Durham, North Carolina 27713
 ^hone: (919) 544-5729 • Fax: (919) 544-5491
                                                                       Printed:! 5:20 09/18H
                                                                                                                21

-------
  Page Ho.

  09/18/97
Listing of S975843B.dbt
Matched <3C Peaks  / Ratio /  Ret. Tin
  Compound/

  M_z.... gc.Log omit Why  ..RT.  OK Ratio Total.Area...  Area.Peak.1.. Area.Peak.2.. Rel.RT Conpound.Na
                                                                                                ID. .  Flags.
328
13C12-TCDD
332-334
332-334
PeCDF
340-342



D












340-342
13C 12 -PeCDF
352-354





352-354
PeCDD
356-358
DC

DC

DC
DC
DC
DC
DC
DC
DC
DC
DC
DC
DC
DC
DC
DC
DC

DC
DC

DC
DC
DC
DC
DC
4
NL
4
NL

SN
SN
SN
SN
SN
SN
SN
3N
SN
SN
SN
SN
SN
SN
WH
1
NL
SN

SN
SN
SN
SN
3
NL
19:39
21:14
21:35
21:41
Peaks
0:00
19:55
21:00
21:13
21:34
0.
RO
RO
•65-0.89
8.95
1.52
0.80
0.80
0.84
Peaks
0:
22;
22
23:
23:
24:
24:
24:
24:
25:
25:
25;
25;
25:
25:
26:
26:
:00
:37
: 51
:25
•49
24
:25
:44
:55
;00
:08
:19
:29
:38
;56
:16
:58
1.
RO
RO
RO
RO
RO

RO
RO
RO
RO
RO
RO
RO
RO

RO
RO
32
0
1
2
1
2
1
2
0
4
1
1
3
0
1
1
0
0
-1.78
.80
.82
.54
.91
.36
.42
.43
.53
.35
.20
. 10
. 14
.95
.14
.56
.91
.90
Peak
0:
23:
24:
24;
24:
25:
25:
25:
:00
:49
:20
42
;52
28
:47
:52
26:27
Peaks
0:
:00
1.
RO
RO
RO
RO
RO
RO
RO
1.
RO
32
1
2
2
1
3
1
7
6
2
32
5
-1.78
.00
.33
.33
.50
.27
.49
.09
.42
.07
-1.78
.60
7
2,615
3
3
2,630
0
7
4.836
3,017
31
7,893
0
8
2
0
8
2
1
1
1
1
0
0
2
3
1
0
0
8
0
3
8
3,116
4
2,822
1
1
4
5,946
P«(T\
> rOL.1/
0
.51 7.51
•91 2,615.91
•24 3.24
.49 3.49
.15
.39
.89 6.76
•79 2,156.40
.80 1,343.17
•45 14.34
.93
D / PeCDF Follows —
.07
•31 5.94
.22
.59
.13
.47
.53
.92
.10
.94
.54
.74
.83
.14
.69
.49
.94
.31
.10
.90
•03 7.33
.31 1,870.46
.97
.10 1,689.29
.43
.53
.82
.44
F / PeCDD Follows —
.13
0.926
1.001 37C1-TCDD SUR1
1.017
1.022
0.906-1.094
0.000
4.46 0.939
2,680.39 0.990 13C12-1234-TCDD RSI
1,674.63 1.000 13C12-2378-TCDD IS1
17.11 1.016

0.905-
0.
3.26 0.
0.
0.
0.
0.
0.
1.
1.
1.
1.
1.
1.
1.
1.
1.
.

0.838-
0,
0.
3.15 0.
1,245.85 1,
1.
1,132.81 1,
1.
1.
1.
0.919-
0.

1.077
000
916
925
948
964
988
989
001 12378-PeCDF AN
009
012
018
025
032 23478-PeCDF AN
038
050
063
092

1.162
000
964
985
000 13C12-PeCDF 123 IS2
007
031 13C12-PeCDF 234 SOR2
044
047
071
1.025
000
Triangle Laboratories, Inc.® Analytical Services Division
801 Caprtola Drive • Durham, North Carolina 27713
Dhone: (919) 544-5729 • Fax: (919) 544-5491
                                                                Printed: 15:20 09/18/97
                                                                             220

-------
Page No.
09/18/97
Listing of  S975843B.dbf
Matched GC  Peaks / Ratio / Ret.  Time
Compound/
M_Z....  QC.Log Omit Why  ..RT. OK Ratio Total.Area... Area.Peak.1..  Area.Peak.2.. Rel.RT Compound.Name..  ID..  Flags.

                                                                               0.923
                                                                               0.928
                                                                               0.935
                                                                               0.949
                                                                               0.956
                                                                               0.977
                                                                               0.985
                                                                               0.996
 356-358

 13C12-PeCDD
 368-370
 368-370
 HxCDF
 374-376
         MK
 374-376
  13C12-HXCDF
  384-386
  384-386
DC
DC
DC
DC
DC
DC
DC
DC
DC
DC
DC
SN 23:50 RO 1.23
SN 23:58 RO 1.28
SN 24:09 RO 0.45
SN 24:31 RO 4.59
SN 24:42 RO 4.00
SN 25:15 RO 0.93
SN 25:27 RO -18.10
SN 25:44 RO 0.36
SN 25:52 1.63
SN 25:58 RO 5.94
WH 26:43 RO 1.10
0 Peaks
1.84
2.65
1.00
1.38
3.39
1.10
0.51
0.31
1.55
0.46
1.76
0.00
1.32-1.78
DC




DC


DC
DC

DC
DC
DC
DC

DC
DC
DC
DC
DC
DC
DC


DC
DC



DC

NL


2

NL


SN
SN

SN
SN
SN
SN

SN
SN
SN
SN
SN
SN
WH
4

NL
SN



SN

0:00 RO
25:50
25:59
Peaks
1.
0:00 RO
27:22 RO
27:31
27:41
27:48 RO
28:22
28:29 RO
28:37 RO
28:43 RO
28:48 RO
29:00 RO
29:12 RO
29:22 RO
29:34 RO
29:44 RO
29:49
29:56 RO
30:04 RO
Peaks
0
0:00 RO
27:30 RO
28:22
28:29
28:59
29:11 RO
29:44
9.14
1.55
1.60

05-1.43
1.03
1.50
1.33
1.22
1.53
1.21
1.49
0.33
2.26
0.98
1.45
0.36
3.63
5.38
1 .01
1.41
3 .40
1.75

.43-0.59
0.32
0.75
0.45
0.49
0.48
0.99
0.48
4 Peaks
0.18
1.755.85
148.96
1,904.81

0.70
5.38
12.08
1.44
1.93
10.85
3.54
0.42
0.43
2.19
3.74
0.14
0.36
0.29
1.41
1.64
0.22
0.27
32.05

2.22
1.25
2,317.24
2,162.06
2,280.64
2.13
1,461.67
8,221.61
                                                         1,066.84
                                                           91.60
                                                          Follows
                                                             3.59
                                                             6.89
                                                             5.94
                                                             2.42
                                                            719.33
                                                            706.30
                                                            735.67

                                                            473.75
                                                                               1.001 12378-PeCDD
                                                                               1.005
                                                                               1.034
                                                                                                     AN
                                                    0.845-1.155
                                                        0.000
                                                689.01   1.000  13C12-PeCDD 123 IS3
                                                 57.36   1.006
                                                    0.955-1.051
                                                        0.000
                                                  2.40  0.961
                                                  5.19  0.966
                                                        0.972
                                                        0.976
                                                  4.91  0.996 123478-HxCDF    AN
                                                        1.000 123678-HxCDF    AN
                                                        1.005
                                                        1.008
                                                        1.011
                                                  1.67  1.018 234678-HxCDF    AN
                                                        1.025
                                                        1.031
                                                        1.038
                                                        1.044 123789-HxCDF    AN
                                                        1.047
                                                        1.051
                                                        1.056
                                                     0.859-1.141
                                                         0.000
                                                         0.965
                                               1,597.91  0.996  13C12-HXCDF 478 SUR3
                                               1,455.76  1.000  13C12-HXCDF 678 IS4  Q
                                               1,544.97  1.018  13C12-HXCDF 234 ALT2
                                                         1.025
                                                 987.92  1.044  13C12-HXCDF 789 ALT1
 Triangle Laboratories, Inc.® Analytical Services Division
 801 Capitola Drive • Durham, North Carolina 27713
 °hone: (919) 544-5729 • Fax: (919) 544-5491
                                                                       Printed: 15:20 09/1JW
                                                                                       22

-------
 Page No.

 09/18/97
Listing  of S975843B.dbf

Matched  GC Peaks / Ratio / Ret.  Time
 Compound/

 M_Z	 QC.Log Omit Why ..RT.  OK  Ratio Total.Area... Area.Peak.1.. Area.Peak.2..  Rel.RT Conpound. Name.. ID., flags.
HXCDD
390-392



K






390-392
13C12-HXCDD
402-404





402-404
HpCDF
408-410





408-410
13C 12 -HpCDF
418-420



418-420
HpCDD
424-426





DC

DC
DC

DC

DC
DC
DC
DC


DC
DC



DC


DC

DC
DC
DC
DC


DC

DC
DC


DC
DC

DC


NL

SN
SN

SN

SN
SN
SN
WH
3

NL
SN



SN
3

NL

SN
SN
SN
SN
1

NL

SN
SN
2

NL
WL

SN


0:00
27:55
28:06
28:11
28:22
28:28
28:37
29:00
29:13
29:30
29:44
Peaks

0:00
28:37
29:08
29:12
29:31
29:51
Peaks

0:00
31:15
31:38
31:44
31:54
32:04
Peak

0:00
31:14
32:07
32:27
32:41
Peaks

0:00
31:13
31:31
31:51
.32:09
1.
RO

RO

RO
RO
RO
RO
RO
RO
RO

1.
RO
RO



RO

0.
RO

RO
RO
RO
RO

0.
RO

RO


0.
RO
RO

RO

	 ADOVe: HXCOF
05-1.43
0.
1.
0.
. 1.
2.
3.
1.
2.
2.
2.
11.

05-
1.
1.
1.
1.
1.
1.

88-
3.
1.
1.
1.
12.
3.

37-
2.
0.
0.
0.
0.

83
35
77
27
98
57
61
66
25
47
32

1.43
54
66
31
14
22
99

1.20
60
02
22
75
00
83

0.51
33
42
72
39
45

,88-1.20
1.
2.
1.
0.
1.
35
15
04
80
07
0.
10.
0.
0.
3.
1.
6.
2.
1.
2.
0.
20.
/ HXCDD Follows --•
27
53 6.04
18
34
65 4.85
86
74 4.85
93
37
67
56
92
0.950-1.014
0.
4.49 0.
0.
0.
1.63 0.
0.
3.01 0.
0.
1.
1.
1.

000
956
962
965
971
975
980
993
001 123678-HxCDD
010 123789-HXCDD
018









AN
AH


0.966-1.034
1.
3.
1,559.
1,605.
2,782.
2.
5,946.
Hvf^ nr
> flX^UL
0.
13.
3.
1.
0.
0.
13.
37
52
21 884.19
00 855.13
46 1.529.14
17
67
t / HpCDF Follows --
51
52 6.34
45
12
08
47
52
0.
0.
675.02 0.
749.37 1.
1,253.32 1.
1.

0.994-
0.
6.68 1.
1.
1.
1.
1.

000
980
998 13C12-HXCDD 478
000 13C12-HXCDD 673
Oil 13C12-HXCDD 789
022

1.044
000
001 1234678-HpCDF
013
016
021
027



SUR4
IS5
RS2




AN





0.936-1.128
0.
871.
0.
508.
1.
39
85 258.15
52
55 143.25
64
1,380.40
: HpCDF / HpCDD Follows —
0.35
3.37
37.00 18.84
1.18
24.66 12.73
0.
613.7X) 1.
1.
365.30 1.
1.

000
000 13C12-HpCDF 678
028
039 13C12-HpCDF 789
046


IS6

SUR5

0.976-1.005
0.
0.
18.16 0.
0.
11.93 1.
000
972
981
992
001 1234678-HpCDD




AH
Triangle Laboratories, Inc.®  Analytical Services Division
801 Capitola Drive • Durham, North Carolina 27713
Phone: (919) 544-5729 • Fax: (919) 544-5491
                                                                  Printed: 15:20

-------
Page No.
09/18/97
Listing o£ S975843B.db£
Matched GC Peaks  / Ratio / Ret.  Time
Compound/
M_2....  QC.Log Omit Why  .,RT. OK Ratio Total.Area... Area.Peak.1..  Area.Peak.2.. Rel.RT Compound.Name..  ID.. Flags.
424-426
                     2 Peaks
                                              61.66
13C12-HpCDD
436-438



436-438

OCDF
442-444
















442-444
OCDD
458-460


458-460
13C12-OCDD
470-472
0.88-1.20
DC
DC

DC



DC
DC
DC
DC
DC
DC
DC
DC
DC
DC
DC
DC
DC
DC
DC
DC
DC


DC

DC


DC
NL
SN

SN
1


NL
SN
SN
SN
SN
SN
SN
SN
SN
SN
SN
SN
SN
SN
SN
SN
SN
0

NL

SN
1

NL
0:
31:
32:
32:
00
28
07
24
RO
RO

RO
6.
7.
1.
0.
36
06
03
34
Peak


0:
31:
31:
32:
32:
32:
33:
33
33
33
33
34
34
34
34
35
35


00
09
29
09
:23
41
:03
:07
:15
:28
:32
:17
:34
:45
-.52
:07
:35

0.
RO


RO
RO
RO
RO
RO
RO
RO
RO
RO
RO
RO
RO
RO
RO

76-
1.
0.
0.
1.
1.
1.
0.

1.02
50
92
81
24
36
92
25
1.15
1.
0,
2
2
1
5
0
0
8
.06
.32
.24
.25
.39
.36
.44
.40
.38
Peaks

0
34
35

:00
:39
:07
0


RO
.76
0
0
1
-1.02
.90
.87
.06
Peak


0
0:00 RO
34:41
470-472

1
.76
1
-1 .02
.63
0.88
Peak
0.
0.
674.
1.
674.
HpCDE

0.
0.
0.
0.
29
35
93
24
93
<

15
23
49
72
0.21
0.
0.
0,
0
0
0
0
0
0
0
0
0
0

0
1,034
0
1,034

.23
.08
.25
.34
.13
.72
.60
.96
.47
.66
.17
.15
.00

.19
.07
.96
.07

0.15
460.83
460.83
                                                          341.73
                                                    0.969-1.031
                                                       0.000
                                                       0.980
                                                333.20  1.000 13C12-HpCDD 678 IS7
                                                       1.009
                                                                    Follows
                                                           479.89
                                                            216.17
                                                     .885-1.115
                                                        0.000
                                                        0.898
                                                        0.908
                                                        0.927
                                                        0.934
                                                        0.942
                                                        0.953
                                                        0.955
                                                        0.959
                                                        0.965
                                                        0.967
                                                        0.988
                                                        0.997
                                                        1.002  OCDF
                                                        1.005
                                                        1.012
                                                        1.026
                                                     0.885-1.115
                                                         0.000
                                                 554.18   0,999 OCDD
                                                         1.012
                                                                             0.994-1.004
                                                                                 0.000
                                                                         244.66  1.000 13C12-OCDD
                                                                                                      AN
                                                                                                      AN
                                                                                                      IS8
 Column Description	   "Why" Code Description	   QC  Log Desc.
  M_Z   -Nominal Ion Mass(es)
  ..RT. -Retention Time (mtn:ss)
  Rat.l -Ratio of M/M+2 Ions
  OK
       -RO=Ratio Outside Limits
  Rel.RT-Relative Retention Time
      End of Report
        WL-Below Retention Time Window  A-Peak Added
         WH-Above Retention Time Window
         SN-Below signal to Noise Level
         
-------
       17:00           18:00           15:00           20:00           21:00          22:00
FllesS975843 #1-848 Acq:ll-SEP-1997 21:04:32 EI+ Voltage SIS 70S NO±fe:857
 05.8987 T:2 BSUB(256,30,-3.0)  PKD(9,5,5,0.05\,3428.0,1.00\,r,T) XzpiXPCOS
TRIANGLE LABS  Text:I-H23-3  TLIf43085                       IW7. TIME -   21:06
ileiS975843 11-848 Aoqtll-SXP-1997 21:04:32 XX+ Voltage SIX 705 Holmei182
03.9016 Ti2 BSUB(256,30r-3.0) PXD(9,5,5,0.05%,728.0,1.OQ\,T,T)  XxpiXPCUB
  IAHCLX LABS  TexttI-M23-3 TLH43085                        IW7. TIME -   21i06
 00*        A1.34X6 A1.65X6
 80:
 60:
 40:
 20:
  0:
                         Al.09X6
       17:00           18:00           15:00           20:00           21:00          22:00
rilesS975843 #1-848 Acqsll-SEP-1997 21:04:32 EH- Voltage SIX 70S Hoimes436
315.9419 T:2 BSOB(256,30, -3. 0) PKD(9,5,5, 0. 05\,1744. 0,1. 00\,T,T) EzpsEPCUS
TRIANGLE LABS  Text:I-M23-3  TLHH3085                       ISJ. TIME -   21:05
1001
 80:
 60:
 40:
 20:
  0:
       17:00           18:00           19-00           20:00           21:00
Tile:S975843  #1-848 Acqsll-SEP-1997 21:04:32 Eli- Voltage SIS  70S No±ae:549
317.9389 T:2  BSUB(256r 30,-3.0)  PKD(9,5,S, 0. 05\,2196. 0,1. 00\,F, T) EzpsEPCOS
TRIANGLE LABS  Text.-I-M23-3 TL1#43085                       IKT. TIKE -   21:06
1001                                                        A2.29E7
  80J
  60:
  40:
  20:
   o:
                                                                                       22s 00
        17:00          18:00           15:00           20:00           21:00
rilesS975843 #1-848 Acqsll-SEP-1997 21:04:32 XI+ Voltage  SIS 70S
330.9792  T:2 XxpsEPCUS
TRIANGLE  LABS  TextsI-M23-3 TLH43085                        IJTJ. TIME '
  80:
  60:
  40:
  20:
   o:
         rr
                         rr
                                                         T
        17:00           18:00           IP.-00            20:00
 rilesS975843 tl-848 Acqsll-SEP-1997 21:04:32 EI+  Voltage SIS 70S
 375.8364 Ts2 ExpsEPCUS
 TRIANGLE LABS  T9Xt:I-M23-3 TLH43085                        UKT. TIMS -
 1001
                                                                        21:00
                                                                                       22:00
                                                                            21:06
                  17s 36
                                           19:14
                                                                               21:30
                            18:14
                                             -3.9X5
                                             .3.1X5
                                             .2.3X3
                                             .1.5X5
                                             .7.7X4
                                                                                                      0.0X0
                                                                                                         Time
                             A3.84X4    A2.64X4
                                   AS.02X4
                                                                                                      4.3X6
                                                                                                      3.5X6
                                                                                                      2.6X6
                                                                                                      .1. 7X6
                                                                                                      .8.7X5
                                                                                                      0.0X0
                                                                                                          Time

                                                                                                      .5.8X6
                                                                                                      .4.7X6
                                                                                                      .3.5X6
                                                                                                      .2.3X6
                                                                                                      .1.2X6
                                                                                                      .0.0X0
                                                                                                          Tim

                                                                                                      .5.8X6
                                                                                                      .4.7X6
                                                                                                      .3.5X6
                                                                                                      .2.3X6
                                                                                                      .1.2X6
                                               0.0X0
                                                  T±m,
                                                                                                      -5.9X3
                                                                                                      '-4. 8X3
                                                                                                      .3.6X3
                                                                                                      .2.4X3
                                                                                                22133
                          1:02
        17:00
                        la'iOO
                                        19\00
20\00
                                                                                         22:04  il  I   :
                                                                                        M-A-Juu/MLj*:
                                                                        21 i 00
22^00
                                                                                                      '.1.2X3
0.0X0
   T±i
                                                                                                      224

-------
 'll»iS975843 tl-848 Aoqill-SKP-1997 21,04*32  EI+  Voltage SIX 70S Jfo±f»,186
 19.8965 r,2 BSUB(256,30,-3.0) PKD(7,5,3,0.05\,744.0,1.00\,r,T)  ExptXPCUS
TRIANGLE LABS  T»xt,I-M23-3 TLIt43085                        JJU. TIME -
                                               A8.69E4
                     19 1 00              20 1 00              21,00
r±lt,S975843 11-848 Aoqtll-SEP-1997  21,04,32 EH- Voltage SI* 70S Noif*,304
321.8936 Ti2 BSOB(256, 30, -3.0) PKD(7, S, 3, 0 .05\, 1216.0,1 .00\,f,T)  XxptXPCOS
TRIANGLE LABS  T»xt, I-M23-3 TLH4308S                        OUT.  TIME -   21t06
      A3. 71X4
                     19,00              20,00               21,00
Fila,S975B43 tl-848 Acqsll-SEP-1997 21,04,32 EH- Voltage SIR 70S Noise:987
331.9368 r,2 BSUB(256, 30, -3. 0)  PXD(7,S, 3, 0. 05\,3948. 0,1.00\,r, T) ExptEPCUS
TRIANGLE LABS  Text:I-M23-3  TLIt43085                       IKJ. TIME -   21:05
100*                                                       A2.16E7
                                                                                  \*'
                                                                               22,00
                                                                               22100
  601

  40:

  20:.

   0.
                                                                 .34E7
                     19 i 00               20,00              21,00
F±le,S97S843  tl-848 Acqtll-SEP-1997 21:04,32 EI+ Voltage SIX  70S Noiee:109
333.9338  T:2  BSOB(256, 30, -3. 0) PXD( 7,5,3, 0. 05\,436. 0,1. 00\,T,T) ExptEPCOS
TS I ANGLE  LABS  TextiI-H23-3 TLH43085                       IW. TIME -
1001
                                                                                22,00
  BO:
  40:

  20:
                                                                 1.67E7
                     19,00               20,00              21,00               22,00
 riletS975843 tl-848 Acqtll-SEP-1997 21,04:32  EH-  Voltage SIR 70S No±»e,139
 327.8847 1,2 BSUB(256,30,-3.0) PKD(7,5,3,0.05%,555.0,1.00\,r,T)  Exp:EPCUS
 TRIANGLE LABS  Text,I-M23-3 TLIt4308S                        IKT.  TIME -   21,06
 1003

  80:

  60l

  40:

  20:
                      19:00              20:00               21,00
 rile,S975843 tl-848 Acqtll-SEP-1997 21,04,32 EH- Voltage SIX 70S
 330.9792 rt2 ElptEPCUS
 TRIANGLE LABS  Teit.sI-M23-3 TLH43085                       IJKT. TIME -
 1001
                              19,26 19,4530,03    20,5  ™>OS 3l!-34
                                                                                22,00
                                                                            21,06
                                                                                22:00
                      19,00
                                          20,00
                                                             21,00
                                                                                 22,00
5.8E6

4.6E6

3.5E6

.2.3X6

1.2E6

.O.OSO
   Time



.7.4X6

.5.9E6

.4.5X6

.3. 0X6

.1.5X6
                                                                                                  0.0X0
                                                                                                     Tim
                                                                                                  6.6X6

                                                                                                  5.3X6

                                                                                                  4.0X6

                                                                                                 .2.6X6

                                                                                                 .1. 3X6
 0.0X0
    Tim
                                                                                                         22!

-------
rlle:S975843 #1-840 Aoq:ll-SEP-1997 21:04:32 EI+ Voltage SIX 708 Xoiae:18
339.8597 Ti2 BSOB(2S6, 30, -3.0) PKD(7,5,3,0.05\,72.0,1.00\,r,T)
Xlp:ETCOS
TRIANGLE LABS Teit:I-M23-3 ZXI #43085 XKJ. TIME " 21:06
IOCS
80:
60:

40.
20:
0
A7. 4X4


A5.94X4
AA1.87X4
\ XI tSft \
A2.21X4 A3 .75X3 V A A7 67E3 In '
AA/^ vAjtfcjs^-A^ ijt^v*** \j»Vj»jrL u-A-A^I^ * WJ^^A / \ PV " A
'23,00 	 24:00 	 25:00





fr07S3*1'lil:4A1.03f4 A6.19X3 1
* il A/ \^J' V^u« t /^/VJL AII ft **- •»- A A>» ^wl y
.3.ir4
.2.514
.1 . 8X4

.1.2X4
.6.2X3
O.O*O
25: 00 T±me
rile:S975843 #1-848 Acqill-SEP-1997 21:04:32 EH- Voltage SIX 70S Holme: 26
341.8567 r*2 BSUB(256, 30, -3.0) PO>( 7,5, 3, 0 .05\,104 .0,1.00\,F,T) XxpiSPCOS
TRIANGLE LABS TextiI-M23-3 TLH43085 IKJ. TIME - 21:06
1001
80J
60J
,

40:
20:
o:
A3.26E4


1 MI iQfA A2.22X4

jT"-f«3 «.««ft A1T4 h\i*9T
JLJ LjuJH_^v_ _ AAX\JWW IMAAM /v'^jWAiAywl
2J:00 ' 24:00 	 25:00
-1.3X4



Al . 67E4
"A-«y|/|A ,A "'fflJii^
.1 . 0X4
.7.8X3


.5.2X3
.2.6X3
O.OTO
26 1 00 Time
rlle:S975843 #1-848 Acq:ll-S£P-1997 21:04:32 EH- Voltage SIX 70S «oiae:29
351.9000 T:2 BSUB(2S6, 30, -3. 0) PKD(7,5, 3, 0. 05\,116. 0,1. 00\,r,T) Exp:EPCOS
TRIANGLE LABS Text:I-M23-3 TLI»4308S IKT. TIME - 21:06
100]
80:
60:
40:
20:
o:
A1.B7X7




J \
2J:00 24:00 25:00
r6.1X6
Al.



J
65JJ7



t
'-4.8X6
'.3 . 6X6
'-2.4X6
.1.2X6
'• 0 . OEO
261-00 	 Time
rile:S975843 #1-848 Acq:ll-SEP-1997 21:04:32 EI+ Voltage SIX 70S Soiae:31
353.8970 T:2 BSUB(256,30, -3 .0) PKD(7,5, 3, 0. 05%,124. 0,1. 00 \,T, T) ExpsEPCUS
TRIANGLE LABS Text:I-M23-3 TLH4308S IWJ. TIME - 21:06
10 OS

80:
60:
401
201
OJ
A1.25E7
I
f\



1 \
23:00 '24:00 ' '25:00
^4.0X6
A1.13E7




	 J




^

.3.2E6
.2.4X6
.1 . 6X6
.8.0X5

	 26:00 	 Time
rile:S975S43 #1-848 Acq:ll-SEP-1997 21:04:32 EI+ Voltage SIX 70S
330.9792 T:2 Exp:XPCUS

TRIANGLE LASS Text: I-M23-3 TLH43085 IlKT. TIME - 21:06
1001
80.
60.
40.
20.
0
24:23
' — ^^r^\ 33&^rJ~^\r**^ r\ C"^
^ \r^ ^ \ v
V V


23:00 24:00 ' 25:00
25:25 26s 14 26:36
A x^^v fv -/\- /^w\ /\ rW^~^S
^^^^/M/v^
\l ^



26-00 	

.5.7X6
.4.3X6
.2.8X6
Ll . 4E6
.0.0X0
rile:S975843 #1-848 Acq:ll-SXP-1997 21:04:32 EH- Voltage SIX 70S
409.7974 7:2 EipiEPCDS

TRIANGLE LABS Text:I-M23-3 TLH43085 IW. TIME - 21:06
100}
80.

60.

40.

20.
0.
25

23:42

33s" 24,43

H 24:11 • I
f^lL. ,. -jJlJuJL ^f^-A^^L Jljv^vu
08 C3.5E3






-A i ^ L«>
If o &E3
f
£.2.11:3
|
E.1.4JTJ
it
25,37 fc5-58 atf)lfl a«,36 J I7'1"
-*AAA>wJLA_A\A — A^x^_A«^/MVE rt «_.,
23:00 24:00 25:00 26:00 Tl*e
226

-------
          24:00                          25:00                         26:00
 ile,S975843 tl-848 Acytll-SXP-1997 21,04,32 EH- Voltage SIS 70S Noil*:25
 57.8516 F:2 BSU3(256,30,-3.0) PKD(7,5,3,0.05\,100.0,1.00\,T,T) ExptEPCUS
TSIAKGLX LABS  T*xt:I-M23-3 TLH43085                       IKT. TIME -   21:06
 003k         Al. 7X4
 .l*iS97584J #1-848 Aoq:ll-SSP-1997 21:0*lJJ 11+ Voltage SIX  70S MOlf*:lJ9
 55.8546 T>2 BSUB(356,30,-3.0) PH>(7,5,3,0.05\,556.0,1.00\,r,T)  XxpiXPCUS
 IAHGLX LABS  T*xt:I-M23-3 TLIt43085                       JW. TINT -   21:06
 001                          AS. 3 2X4
 so:
          24:00                         25:00                         26:00
 •±le:S975843  U-848 Acq:ll-SEP-1997 21:04:32 EI+ Voltage SIS  70S No±ae:320
 67.8949 t:2  BSUB(256,30,-3.0) PKD(7,5,3,0.05\,1280.0,1.00\,r,T) Exp:EPCUS
TBIANGLE LABS  Text:I-M23-3 TLIt430SS                       IKT. TIME  -  21:06
 001                                                            Al  07E7
  80.

  so:

  40.
  20:
                                                                      19.16E5
                                                                       /\	
          24:00                          25:00                         20:00
 rlle:S975843 #1-848 Acq:ll-SEP-1997  21:04:33 EI+  Voltage SIX 70S Noise-.35
 369.8919 Ts2 BSUB(256,30, -3. 0) PKD(7,5,3, 0. OS\,140. 0,1. 00\,T, T) Exp:EPCOS
 TRIANGLE LABS  Teit:I-M23-3 TLI043085                        IJKT. TIME -   21:06
 1003

  so:

  50.

  40:

  20.
                                                                 A6
                                                                    B9E6
                                                                      \S. 74ES
                                                                       TV
           24,00                         25:00                         26:00
 File:3975843 #1-848 Acq:ll-SEP-1997 21:04:32 £1+ Voltage SIR 70S
 330.9792 T:2 ExptEPCUS
 TRIANGLE LABS  Text:I-M23-3 TLH43085                       IJKT. TIMX  -   21:06
                                                      25125
1003

 801

 so;

 40.

 20:

  0.
                       24:23
                                         34,59  35,13
           2400
                                          25tOO
                                                                        26,00
                                                                                                -3.4E6




                                                                                                -2.0E6

                                                                                                .1.4X6

                                                                                                .6.8X5
                                                                                                 O.OEO
                                                                                                    Time
                                                                                                 2.2X6

                                                                                                .1. 8E6

                                                                                                .1.3X6

                                                                                                .8.8X5

                                                                                                -4.4E5
                                                                                                 ,0.0X0
                                                                                                     Time
.7.1X6

.5.7X6

.4.3X6

'.2.8X6

-1.4X6

.0.0X0
                                                                                                           22

-------
f±l», 3975843 11-405 Aoqill-SXP-1997 21i04i32 XI+ Voltage SIX 70S Holm* t 194
373.8308 fi3 BSUB<256, 30, -3.0)  PXD(7,3,3r0.05\,776.0,1.00\,r,T) XxptOCOS
TXIANGLX LABS  Text:I-M23-3  TLIt430S5                       IW. TIM* -   21i06
1005

 40:

 60:

 40.

 20.
           A6.89X4
       A3.59X4,
                                       AS. 94X4,
                            A1.53X4
       4
                                                           A4.64X4
     AS. 79X3
           A6.98X3*?-5"3
.02X3   R      i    Jt f#3.38X3
                 AA/*V-JM«Jt .A-—:
                                                                                                      0.0X0
                                         28i24 ' 28:36  28'i48  29^00 29>12 29t24  29i36 29', 48 30iOO  30tl2   Tim,
                                                                                                     .2.4X4

                                                                                                     '•.1.9X4

                                                                                                     .1.4X4

                                                                                                     .9.5X3

                                                                                                     .4.8X3
         27:2< 27i36
rlle:S975843 tl-405 Acqill-SXP-1997 21:04:32 XI+ Voltage SIX 70S Noime:190
375.8178 T:3 BSUB(256,30,-3.0)  PXB(7,5,3,0.05\,760.0,1.00\,r,T) XzptXPCOS
TXIANGLX LABS  \Text:I-M23-3  TLIt43085                       IKT. TIMX -   21:0*
                                      A4.91E4
   27\12  27\24' 27:36 27':48  28:00 28': 12 28':24  28\36 2B\48 29:00 29112  29:24 29:36 29:48  30:00 30:12   Time
 rile:S975843 fl-405 Acq:ll-SEP-1997  21:04:32 EI+ Voltagre SIX 70S Holme:377
 383.8639 T:3 BSUB(256,30,-3. 0) PKD(7,5,3, 0. 05\,1508.0,1. 00*,r,T) Exp:XPCUS
 TRIANGLE LABS  Text:I-M23-3 TLH43085                        HKT. TIMX -
                                       A7.19X6             *7 36E6
 lOOi
  80:
  so:
  40:
  20:
   o.
                                                                                  A4.74X6
                                                                                                     .2.3X6

                                                                                                     -.1. 8X6

                                                                                                     '-.1.4X6

                                                                                                     _5.1X5

                                                                                                      .4.6X5

                                                                                                      .0.0X0
    27:12' 27:24'27\36~ 27,46 28:00 28:12  28:24  28:36 28:48  29:00  29:12 29:24 29:36  29:48 30:00 30:12   Tim
 r±le:S975843 tl-405 Acq:ll-SEP-1997 21:04:32 EH- Voltage SIX 70S Woiaa:1172
 385.8610 T:3 BSUB(256,30, -3 . 0)  PKD<7, 5,3, 0. 051,4688. 0,1. 00\,T, T) Xxp:EPCVS
 TRIANGLE LABS  Text:I-M23-3  TLI#43085                       IKT. TIME -   21:06
 1003

  80:

  60:

  40.

  20.

   o:
    27:12 27:24 27:36  27:48 28:00 28:12  28:24 28:36 28:48  29:00  29:12
 File:S975843 tl-405 Acq:ll-SEP-1997 21:04:32 EI+ Voltage SIR  70S
 392.9760 T:3 ExpsEPCCS
 TRIANGLE LABS  Text:I-M23-3 TLIt43085                       IKJ. TIME
 100J|    27:22   27f.?7	2JLL05 38JJ-7               28:55
                                           60X7
                                                           Al
                                                              54X7
                                                                                   A9.88E6
                                                                                                      .4.7X6

                                                                                                      L3.7E6

                                                                                                      .2.8X6

                                                                                                      .1.9X6

                                                                                                      .9.3X5

                                                                                                       0.0X0
                                                                         29:24  29:36 29:48 30:00  30,12  Tim
                                                                             21:06
                                                                           29:27
                                                                                                      _.3 . 7X6
                                                                                                        O.OEO
    27:12  27:24 27:36 27:48  28:00 28:12 28:24  28:36 28:48 29:00  29:12
  F±le:S975S43 tl-405 Acq:ll-SEP-1997 21:04:32 EI+ Voltage SIR 70S
  445.7555 F:3 Exp:EPCUS
  TRIANGLE LABS  Text:I-M23-3 TLIt43085                       IKT. TIME -   21:06
                                                                                                       LO.OJTO
    27:12 27:24 27:36  27:48 28:00 28:12  28:24 28:36 28:48  29:00 29:12 29:24 29:36  29:48 30:00 30:12   Tim
                                                                                                         228

-------
riJ.*,SS75B1J tl-405 Aoqtll-SXP-1997  21tQ4t32  Mir Voltage SIM 70S HOiaei74
389.8156 Ti3 aSU*(256,30,-3.0) PKD(7, 5,3,0.05\,296.0,1.00\,r,T) Xxp,XPCUS
TRIAHGLX LABS  Text,I-M23-3 TLH4308S                        IKT. TIM* '   21*06
         A6.04X4
            (V
                                    .1.7X4
      37:48   23,00    28:12   28,24   28s 36   28s 48    29,00   29,12   29,24    29', 36   29,48
Tile:S975843 11-405 Acqtll-SXP-1997 21:04,32 XII- Voltage SIX 70S Holae:88
391.8127 Ti3 BSOB(256,30,-3.0) PXD(7,5,3,0.05\,352.0,1.00\,r,T> XzptXTCUS
TRIANGLE LABS   Text:I-M23-3 TLIt43085                       IXT. TIMX  -   21,06
1001     A4.49E4

  so:
      27:48    38:00   28,12   28:24    28,36   38,48   39,00   29,12   29,24   29,36   29:48
 rlle,S975B43 tl-405 Acqtll-SEP-1997 21,04,32 EI+ Voltage SIR 70S No±ae,471
 401.8558 r,3 BSUB(356,30,-3.0) PKD( 7, 5, 3, 0. 05\,1884. 0,1. 00%, F, T) KxptEPCVS
 TRIANGLE LASS  Text:I-M23-3 TLIt43085                        IKT. TIME -   21:06
 1004                                                                       A1.5.3E7
  so:

  60.

  40:

  20.
A8.84E6
                                                                                                  0.0X0
                                                                                                     T±mt
.3. 8X6

.3.1X6

.2.3X6

.1. 5E6

.7.7X5
       27,48   28:00   28', 12    28:24   28,36   28:48    29:00   29', 12   29:24    29,36   29:48
 rile:S975843 #1-405 Aoqtll-SEP-1997 21,04:32 EI+ Voltage SIR 70S Hoiaf.305
 403.8529 r,3 BSUS(2S6,30,-3.0)  PKD(7,5,3,0.05\,1220.0,1.00\,T,T) ExpsEPCOS
 TRIANGLE LABS  TextsI-H23-3  TLH43085                       IKJ. TIME -   21:06
 1004                                                                        A1.25E7
                                     .0.0X0
                                         Tine
   80J

   so:

   40:

   20:
A6.75E6
-3.2X6

 .2.6X6

 .1.9X6

 .1.3X6

 .6.4X5
       27\48  ' '28t6o   28,12   28:24    28:36   28,48   29,00   29il2   29:24   29:36   39,48
  File:3975843 tl-405 Acqill-SXP-1997 21,04:32 XI+ Voltage SIR  70S
  392.9760 T,3 XxptXPCUS
  TRIAHSLX LABS  T»xttI-H23-3 TLI»43085                       IXJ.  TIMX -   21:05
  100J

   80.
                                      ,0.0£0
                                         T±me
                                                                                                   0.0X0
       '27l:48 '  '28i00   28:12    28:24   28:36   28:48    29tOO   29tl2   29,24    29:36   29:48
                                                                                                       229

-------
 il*:S975843 tl-430 Acqtll-SXP-1997 21:04:32  11+  Voltage SIX 70S Moi*et452
 07.7818 r>4 BSDB(2S6,30,-3.0) PKD(7,5,3,0.05\,1808.0,1.00\,T,T) XxpiXPCUS
TXIANGLX LABS  TexttI-M23-3 TLH43085                        ZK7. TIMX -   Hi06
 004    A3.16X5

 ao:

 60:

 40:

 201
  31iOO      31:12     31:24     31:36     31:48      32:00     32:12     32:24     32:36
 lletS975843 tl-430 Acqtll-SXP-1997  21:04:32  XI+ Voltage SIX 70S Noi*e:125
 09.7789 Ts4 BSOB(256,30,-3.0) PKD(7,5,3,0.05\,500.0r1.00\,r,T) XxpiXPCUS
TMIAXGLX LABS  Text:I-M23-3 TLIt43085                        IJKT. TIMX -   21s 06
  004         A6.68E4

  80:

  60:
             A6.84E4
                                                                                              32:48
40:

20.
                               A1.69S4

                                                                        A1.55E4  A6.66E3
                                              **
  31,00     31:12      31:24     31:36     31:48     32:00      32:12     32:24     32,36
f±10:3975843  tl-430 Acqsll-SEP-1997 21s04s32 EH- Voltage SIX  70S Noiae:313
  17.8253 T:4  BSUB(256r30,-3.0) PKD(7,5,3,0.OS\,1252.0,1.00\,T,T) SxpsEPCUS
TRIANGLE LABS  Text:I-H23-3 TLH4308S                       INJ. TIME -   21:06
1004         A2.58E6

  ao:

  60:
  40-           I  \                                                         A1.43E6

  20:
                                                                                              3248
  31:00      31:12     31:24     31:36     31:48      32:00      32:12     32:24
 rilesS975843 tl-430 Acqsll-SEP-1997 21:04:32  EI+  Voltage SIS 70S Noiae:135
 419.8220 r:4 BSUB(256, 30, -3. 0) PKD(7, 5,3, 0. 05\,540. 0,1. 00\,T,T) ExpsEPCUS
 TRIANGLE LABS  Text:I-M23-3  TLIt43085                       HKT. TIME "   21:06
 1004        A6.14E6

  80:

  60:

  40:

  20:
                                                                                    3236
                                                                                              3248
                                                                            A3.65X6
   31  00     31:12     31:24     31:36      31:48     32:00     32:12
 rilesS975843 tl-430 Acqsll-SEP-1997 21:04:32 EI+ Voltage SIX 70S
 430.9729 r:4 ExpsEPCUS
 TRIANGLE LABS  TextsI-M23-3  TLIt43085                        IJTJ. TIME -
 1004
 *w ^     •* i - no  .~.*,*         . — £_—•—_         . . .. 4r.«tn                . . ,..

   80J

   60:

   40:

   20:
                                                                          3224
                                                                                    32:36
                                                                            21s 06
                                                                                                   .1.1X5

                                                                                                   -8.8X4

                                                                                                   -6.6X4

                                                                                                   .4.4X4

                                                                                                   .2.2X4
                                                                                                      0.0X0
                                                                                                         Tim,
^.2.4X4

.1.9X4

.1.4X4

'.9.5X3

-4.7X3
                                                                                                   LO.OEO
                                                                                                        Tim,
                                                                                                     -6.8ES

                                                                                                     '-5.5X5

                                                                                                     '-4.1X5

                                                                                                     "-2.7XS

                                                                                                     .1.4X5
                                                                                                     0.0X0
                                                                                                        Tim:
                                                                                                   ^1. SE6

                                                                                                   -.1.2X6

                                                                                                    .8.9ES

                                                                                                   '-..6.0X5

                                                                                                   Lj.0X5
                                                                                              32:48
                                                                                                    LO.0X0
                                                                                                        Tim
   0:
                                                                                                     ^2.4E6

                                                                                                     -1.9E6

                                                                                                     .1. 4X6

                                                                                                     .9.6X5

                                                                                                     -.4.8X5
   31-00     31:12      31:24      31:36     31,48     32:00     32,12      32:24
 rile:S975843  tl-430 Acqsll-SEP-1997 21:04:32 EI+ Voltage SIX  70S
 479.7165 Ts4  ExpsXPCUS
 TRIANGLE LABS  TextsI-M23-3 TLH43085                       INJ. TIME -  21:06
 1004                    31:26
                                                                                    3236
                                                                                               3248
                                                                                                     O.OEO
                                                                                                        Tim
   31:00
             3l:12
                                                                                    32t36
                                                                                               32t48
                                                                                                          Tim
                                                                                                       230

-------
             41-4J0 AoqiJ.l-SfP-1997 21,04,32 XI + VOJ.C*ye SIX 70S HoiM»lllJ
423.7766 T>4 3303(256,30,-3.0)  tXD(7,5,3,0.051,452.0,1.00\,r,T) txptXTCOS
TXIAHSLX LA33  T«xtiJ-«3-J  TU443085                       XK7. TZNT -   2it06
1001               A1.88E5
    31il8   31:24  31i30  3l',36   31,42  31,48  31tS4  32tOO   32,06  32,12  32,18   32,24
rile,S975843  tl-430 Acqill-SEP-1997 21,04,32 XI* Voltfye SIX  70S Half*,83
425.7737 Tit  3303(256,30,-3.0) PKV(7,5,3,0.05\,332.0,1.00\,r,T) ExptEPCUS
TXIAlfSLS LABS  Text:I-M23-3 TLH43085                       INJ. TIME -   21,06
1001              A1.82E5
                                                                                           33,30
  80.

  eo:

  40.

  20:
                                                               A1.19ES
                                              A7.47X3
                                                 A A
                                                                                   A3.07E3
LJ. 3E4

-2.5E4


.J..7E4

.8.3E3
    31:18  31,24   31,30  31,36  31:42   31:48  31:54  32,00  32,06   32,12  32,18  32:24
File:S975843 tl-430 Acq:ll-SEP-1997 21,04:32 EI+ Voltage SIX 70S No±ae,445
435.8169 r,4 BSUB(256,30,-3.0)  PKD(7,5,3,0.05\,1780.0,1.00\,f,T) ExpiEPCDS
TXIANGLE LABS  TeJCt,I-M23-3  TLIf43085                       IXT. TIKE  -   21:06
1001                                                           A3.J2E6

  so:

  so:

  40.

  20:
                                                                                                  .O.OEO
                                                                                            32', 30    Time
                                                                                                  5.5E5

                                                                                                  .4.4E5

                                                                                                  .3.3E5

                                                                                                  '.2.2E5

                                                                                                  11. 1E5
                                                                   3E6
     31,18   31,24  31,30  31:36   31,42  31,48  31,54   32:00   32:06  32,12
rila,S975843  tl-430 Acgill-SEP-1997 21,04,32 EH-  Voltage SIX 70S NOiae:70
437.8140 T:4  BSOB(256,30,-3.0) PKD(7,5,3,0.OS\,280.0,1.00\,r,T)  ExpiEPCDS
TXIAKSLE LABS  Text,I-M23-3 TLIt43085                        IJKT. TIME -   21:05
1004                                                          A3.
   so:

   eo:

   40:

   20:
                                                                              32:IB  32,24
                                                                                                  .O.OEO
                                                                                             32:30    Time
 .5. 6E5

 -4.5E5

 "-3.4E5

 .2.2E5

 .1.1E5
      JlilS  3l'i24  3l':30   31:36  3l',42  3l',48   31,54   32,00  32:06  32,12   32,18  32,24
 r±le,S975843 tl-430 Acqsll-SEP-1997  21:04,32 E1+ Voltag* SIX 70S
 430.9729 r,4 EfptEPCUS
 TXIANSLE LABS  Text,I-H23-3 TLH4308S                        TOT. TIME -   21,06
  1003,                 31ji33                        ,,.-,„
                                            31,49   2t^° —_       ,,.,„       32>20

   soJ

   60.

   40.

   20.
                                                                                                  .O.OEO
                                                                                             32,30    Time
                                                                                                  .2.4X6

                                                                                                  ".1.9E6

                                                                                                  -1.4E6

                                                                                                  -P.5JC5

                                                                                                  .4.8E5
                                                                                                    O.OEO
             '31*24 ' '3'l:30 '  '31t36 ' '31\42 ' '31,48 ' '31,54 ' '32\00 ' '32\06   32tl2  32tl8  32t24   32i30    Time
                                                                                                          231

-------
ro

-------
nj.»,S975843 tl-430 Actj:ll-SEP-1997 21104132 XI+ VOJLCAgm SIX 70S Nol**:43
457.7377 Tt4 BSU*(256,30,-3.0) PXD(7,5,3,0.OS\,172.0,1.00\,r,T) XxptXtCOS
TRIANGLE LABS  TmxttI-M23-3 TLH43085                        HKT. TIM* -   21tO«
1001

 80.
           34t30         34i36         34:42        34,48         34:54
r±lftSS75843  91-430 Acqtll-SEP-1997 21:04:32 XI+ Voltmgm SIX 70S Ko±f»:48
459.7348 Ttt BSUB(256,30,-3.0)  PXB(7,5,3,0.05\,192.0,1.00\,T,T) XxptEPCOS
TRIANGLE LASS   T*xt:I-M23-3  TLH43085                       IJKT. TIMS -   21:06
1001                               AS.
                                                                                35100
            34:30         34:36        34,42         34,48         34:54
 rile,S975843 tl-430 Acq:ll-SEP-1997  21:04,32 £1+ Volts ye SIR 70S JfOim«:40
 471.7750 T,4 BSOS(256,30,-3.0) PKD(7,5,3,0.05\,160.0,1.00\,f,T) ExpiSPCUS
 TKI ANGLE LASS   Text: I-M23-3  TLH43085                       IKJ. TIME -   21:06
           34:30         34,36         34:42         34:48        34,54
 r±le>S975843 tl-430 Acqsll-SEP-1997 21:04:32 EI+ Voltage SIX  70S Xoiee:64
 469.7779 T,4 BSUB(256,30,-3.0) PKD(7,5,3,0.05\,256.0,1.00\,F,T) ExpiEPCUS
 TRIANGLE LABS  Text:I-M23-3 TLI943085                       INJ. TIME '   21:06
 100S,                               A2.J.6E6
  so:

  60.

  40:

  20:
                                                                                35,00
                                                                                 35,00
 1001
   so:
                                      A2.45E6
            34:30         34:36         34,42         34:48         34:54
 rile:S97S843  11-430 Acqtll-SEP-1997 21:04:32 EI+ Voltage SIS 70S
 430.9729  T:4  ZxpiEPCUS
 TRIANGLE  LABS  Toxt:I-M23-3 TLH43085                       IJKT. TIME -
                                                                                 35:00
                                                               21:06
  ion

   so:

   «o:

   40.

   20.

    0.
34:30
                            34,42
                                                                                 33 Of
                                                                                                 .4.9*3


                                                                                                 '.4.0X5

                                                                                                 -3.0X3

                                                                                                 .2.0E5

                                                                                                 -9. 9E4
                                                                                    .O.OEO
                                                                                 35 06  Tim.
                                                                                    -2.1E5

                                                                                    .1. 7E5

                                                                                    -1.3E5

                                                                                    .8.5E4

                                                                                    -4.2S4
                                                                                    .O.OEO
                                                                                 35 06  T±m
                                                                                  35
.1. 0X5

-1.3E5

'.9.0X4

14.5E4

.O.OEO
 06  TiM



.2.7X6

'.2.1X6

'.1. 6X6

.1.1X6

^5.3X5
            34130
                          34:36
                                        34:42
                                                      34,48
                                                                    34,54
                                                                                 35100
                                                                                     .0.0X0
                                                                                  35 06  Urn
                                                                                                       233

-------
ChameL    I  338,9792     Peak top
Height   1,51 vdts  Span   299 ppi
Systei file naie
Data   file naie
Resolution
Group nunber
lonlzatlon node
Switching
Ref, lasses   292,
fl   293      J   331
B   304
C   386
0   318
E   318
F   329
G   322
H   328
I   331
K   332

*   349
N   342
0   352
P   354
Q   356
R   358
               EPCUS
           fl=S975843
      2
     El*
 VOLTflGE
416,9768
S   368
T   379
U   376
V   418
 Ref, aass    416.9768    Peak top
 Height   ,27 volts  Span  298 ppi
                                                       234

-------
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-------
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-------
TLI Project:      43085
Client Sample:   I-M23-3
               Method 23 TCDD/TCDF Analysis (DB-225)
                                    Analysis File:   P973854
Client Project:
Sample Matrix:
TLI ID:

Sample Size:
Dry Weight:
GC Column:

Analytes •:'•"•' ..•'.. •"•

S413-004
M23Train
181-55-7ABD

1.000
n/a
DB-225

•v^l^;--./-r: Amt


Date Received:
Date Extracted:
Date Analyzed:
Dilution Factor:
Blank File:
Analyst:

(ng) Dt


09/03/97
09/04/97
09/12/97
n/a
P973852
ML

EMPC


Spike File:
ICal:
ConCal:
% Moisture:
% Lipid:
% Solids:

Ratio


SPC2NF04
PF22206
P973843
n/a
n/a
n/a

JTT £faos

2,3,7,8-TCDF
   ND
0.03
 Internal Standard
Amt.;(hg)
           QC Limits -:' n • HRatlit>-
13C,,-2,3.7,8-TCDF
   2.2
   53.9
40%-130%
                                                                    0.74
                                                 20:42
 Recovery Stendafd
13C12-1,2,3,4-TCDD
                                                                    0.80
                                                 19:45
                      Data Reviewer.
             i t i -L_Ll
                                                                09/18/97
                                          Page 1 of 1
                                                                              ONF.PSR Y2.00. LARS 6.10.04
 Triangle Laboratories, Inc.®
 801 Caprtola Drive • Durham, North Carolina 27713
 Phone: (919) 544-5729 • Fax: (919) 544-5491
                                              Printed: 15:53 09/18/97
                                                         238

-------
                       Initial
                                    ..Date..
Data Review By:
                                              Calculated Noise Area:   1.29
The Total Area for each peak with an ion abundance ratio outside
ratio limits has  been  recalculated according to method requirements.
Page No.
09/18/97
Listing of P973854B.dbf
Matched GC Peaks /  Ratio  / Ret. Time
Compound/
M_Z.... QC.Log Omit Why ..RT.  OK .Ratio Total.Area... Area.Peak.1..  Area.Peak.2..  Rel.RT Compound.Name.. ID.. Flags.
TCDF
304-306
 304-306
0.65-0.89
DC
DC
DC
DC
DC
DC
DC
DC
DC
DC
DC
DC

ML
SN
SN
SN
SN
SN
SN
SN
SN
SN
SN
SN
0
0:
17:
19:
19:
20:
20:
20:
20
21
21
22
22
00
36
26
33
13
:21
:43
:57
:37
:45
:14
:25

RO
RO
RO
RO


RO
RO

RO

0.
0.
0.
0.
0.
0,
0
1
1
0
0
0
74
56
47
29
.50
.83
.66
.45
.03
.69
.27
.77
Peaks
1.
0.
1.
0.
0.
1.
4.
1.
0.
1.
0.
58
80
70
57
53
65
48
31
69
.62
,67
0.94
0
.00
                                                    0.786-1.096
                                                        0.000
                                                        0.850
                                                        0.939
                                                        0.944
                                                        0.977
                                                        0.983
                                                        1.001 2378-TCDF
                                                        1.012
                                                        1.044
                                                        1.051
                                                        1.074
                                                        1.083
 13C12-TCDF
 316-318
 316-318
                               0.65-0.89
                 DC  NL
                 DC   SN
 0:00 RO
20:42
21:10 RO
Peak
                                  1.04
                                  0.74
                                  1.25
  2.00
479.31
  0.50
479.31
203.80
    0.952-1.048
        0.000
275.51  1.000 13C12-2378-TCDF ISO
        1.023
                                       Above: TCDF / TCDD Follows
 13C12-TCDD
 332-334
  332-334
0.65-
DC
DC


DC
DC
DC

NL
SN


SN
SN
SN
2
0:
18:
19:
19:
20
21
21
00
:27
31
45
:24
:03
:11
RO
RO


RO
RO
RO
1.
0
0.
0
0
1
2
•0.89
45
.52
.80
.80
.62
.44
.44
Peaks

2.
2.
356.
640.
3,
0
0
997

04
37
36
.64
.36
.69
.32
.00
                                                            158.38
                                                            285.36
                                                     0.897-1.103
                                                         0.000
                                                         0.945
                                                 197.98  1.000 13C12-2378-TCDD IS1
                                                 355.28  1.012 13C12-1234-TCDD RSI
                                                         1.045
                                                         1.079
                                                         1.085
  Column  Description.
         "Why" Code Description	   QC Log  Desc.
  M_Z   -Nominal  Ion Hassles)
  ..RT.  -Retention  Time  (mm:ss)
  Rat.l  -Ratio of M/M+2  Ions
  OK    -RO=Ratio Outside Limits
  Rel.RT-Relative Retention Time
      End of Report
                                 WL-Below Retention Time Window  A-Peak Added
         WH-Above  Retention Time Window
         SN-Below  signal  to Noise Level
         
-------
ro
.£*
o
                                                                                                                                                                                                    a   to   »ovj>-.Oio
-------
 ULuiPS7j854 #1-755 Acq>ll-SEP-1997  19:51,06 fir VoltAg* SIM TOP NOlfflJlo
 03.9016 BSUB(2S6,30,-3.0) PKD(5,3,1,0.10\,1344.0,0.00\,T,T) Exp:DB225
TXIAHGLX LABS  TtxttI-H23-3 TU143085
 00\                                                          Al. 78X4
            17100         IttOO         19100        20,00         21,00
 ile,P9738S4 tl-755 Aoq,12-SEP-1997 19,51,06 EI+ VoltMfff SIX 70P No±f»:453
 05.8987 BSOB(256,30,-3.0)  PXD(5,3,1,0.10\,1812.0,0.00\,r,r) X*p,DB225
TRIANGLE LABS  TextsI-M23-3 TLH43085
                                             A1.57E4          A2.70X4
22100
             17:00         18:00         19:00         30': 00        21': 00
 F±le:P973854 #1-755 Acgsl2-SEP-1997 19,51:06 EH- Voltage  SIS  70P KO±ae:583
  15.9419 BSUB(256,30,-3.0) PKD(5,3,1,0.10\,2332.0,0.00%,T,F)  Exp:DB225
 TRIANGLE LABS  Text.!I-M23-3 TLI#43085
 100\                                                         A2.04E6
  801

  so:

  401

  201
22:00
             17:00         18,00        19,00         20:00         21:00
 rile:P973854 #1-755 Acq,12-SEP-1997  19:51:06 EI+ Voltage SIX TOP Noiae:566
 317.9389 BSUB(256,30,-3.0) PKD(S,3,1,0.10\,2264.0,0.00\,T,T) Exp,DB225
 TRIANGLE LABS  Text:I-M23-3 TLH4308S
 10 OS,                                                          A2.76E6
  80.

  60.

  40.

  201

    0.
                                                                                 22:00
             17:00         18:00         19:00        20:00         21:00
 rile:P9738S4 tl-755 Acqil2-SEP-1997 19:51:06 EI+ Voltage SIX 70P
 375.8364 Exp:DB22S
 TRIANGLE LABS   Text:I-M23-3 TLH43085
  1004
             17tOO
                           18iOO
                                         19,00
                                                       20100
                                                                    21:00
                                                                                  32100
                 6.1E5

                 4.9X5

                 3.7E5

                 .2.SE5

                 .1.2X5
                  0.0X0
                     Tim
                  7.SE5

                 .6.2X5

                 .4.7X5

                 .3.1X5

                 ;.!. 6X5
                  .0.0X0
                     T±a
                                                                                21:53
                                                                 20:47  21:15 al-'°
                                                                                                        241

-------
 20.
                   18:00             19:00             20:00             21:00
 ile:P973854 #1-755 Acqtl2-SKP-1997  19:51:06 XI* Voltage SIX 70P Noil*:501
 21.8936 BSUB(256,30,-3.0) PKD(5,3,1, 0.10\,2004.0, 0. 00\,r,F) Elp:DB225
TRIANGLE LABS  TextiI-H23-3 TLH43085
 001
             tl-755 AOIJIH-BKP-i997 19151:06 fl+ VOJ.Cage 31* 70P W>A*«f
  9.8965 BSUB(256,30,-3.0) PXD(5,3,l,0.10\,1612.0,0.00*,r,r) Xxp:DB225
  TAMCU LABS  TfXt:I-M33-3 TLH43085
                   18', 00              19:00             20:00             21:00
File:P973854  #1-755 Acq:12-SEP-1997 19:51:06 EH- Voltage SIR 70P SOisai523
327.8847 BSUB(256,30,-3.0)  PKD(5,3,1,0.10\,2092.0,0.00\,r,T) Exp:DB225
TRIANGLE LABS  Text:I-H23-3 TLH43085
1001                                          A3.14E6
  801

  601

  40:

  20:
                    18:00              19:00             20:00             21:00
 rile:P973854 #1-755 Acq:12-SEP-1997 19:51:06  EH-  Voltage SIR 70P Noises S3 6
 331.9368 BSUB(256,30,-3.0) PKD( 5, 3,1, 0.10%, 3344 . 0, 0. 00\,f,F) Exp:DB225
 TRIANGLE LABS  Text:I-M23-3 TLI143085
 1001                                              A2.85E6
  80.
  60.

  401

  20.
A1.58E
                    18sOO             19:00              20:00              21:00
 rile:P973854 #1-755 Acq:12-SEP-1997 19:51:06 EI+ Voltage SIX 70P Noi*e:577
 333.9338 BSUB(256,30,-3.0) PXD(5,3,1,0.101,2308.0,0.00\,T,r) Ezp:DB225
 TRIANGLE LABS  Text:I-M23-3  TLH43085
 1001
  80.
  60.

  40.


  20.

   0.
A1.98EI
                    18.00
                                       IPtOO
          50iOO
                                                                           21:00
                                             22100
                                              22:00
                                              22:00
                                              33:00
                                                                                             22,00
                                                       a. ar5

                                                       7.115

                                                       .5.JE5

                                                       .3.5E5

                                                       .1. 8E5
                                                        O.OEO
                                                           Tim
8.4X5

6.7E5

.5.0X5

.3.3X5

.1.7X5
.O.OEO
    Tim
 1. 0X6

 8.3X5

 .6.2X5


 .4.1X5

 .2.1X5
 0.0X0
    Tim
                                                                                                         242

-------
 lie:P973854 #1-755 Aoq:12-SEP-1997 19:51:06 11+ Voltage SIM 709
 03.9016 Exp:DB225
TRIANGLE LABS  Text:I-M23-3 TLH43085
                                                               30143

                                   ...41     1*,,*        "I"  /I    31'i3
                      17:45
            17(00         18:00        19:00         20:00         21:00
 iletP973854 tl-755 Aoj:12-SXP-1997 19:51:06  11+ Voltage SIS 70P
 15.9419 Xxp:DB225
TRIANGLE LABS  Text:I-M23-3  TLH43085
 00*                                                           20i42
 80:
 sol
 40.
 20:
   0.
            17:00         18:00         19:00         20:00         21:00
rlle:P973854  tl-755 Aoq:12-SEP-1997 19:51:06 EI+ Voltage SIR 70P
'19.8965  Exp:DB225
TRIANGLE  LABS  Text:I-M23-3 TLI#43085
100$
       1S,37     17:18   ., ,,     18:35        19:31
                                                                               22:00
             17:00        18:00         19':00         20:00         21:00
 F±le:P973854 tl-755 Acq:12-SEP-1997 19:51:06 EI+ Voltage SIR  70P
 331.9368 Ezp:DB22S
 TRIANGLE LABS  Text:I-M23-3 TLHH3085
 1001                                             IS;
                                                                                22:00
  80J
  601
  40:
  20.
   ol
                                              19:3
            17:00         18,00        19:00         20:00         21:00
rile:P973854 #1-755 Acq:12-SEP-1997 19:51:06  EH- Voltage SIR 70P
292.9825 Eip:DB225
TRIANGLE LABS  Text:I-M23-3  TLI#43085
                                  18:3518:58       19:50
                                                                                 22:00
                                                               6.2*3
                                                               5.0X5
                                                               3. 7X5
                                                               2.5E5
                                                               .1.2ES
                                                               .O.OEO
                                                                  T±m»
100J
 80:
 60:
 40.
 20:
  0:
              17:03
                       17:43
                                          -r
                                                                     ~r
             17:00         18:00        19:00         20:00         21:00
 rile:P973854 #1-755 Aog:12-SEP-1997 19:51:06 EH- Voltage SIR 70P
 330.9792 Exp:DB225
 TRIANGLE LABS  Teit:I-M23-3  TLXJ43085
                                                    19:5020:14 20:41
                                                                                '22': 00
                                                               8.4E5
                                                               6.7E5
                                                               5. 1E5
                                                               3.4E5
                                                               1. 7E5
                                                               .O.OEO
                                                                  Tim


                                                               .5.3E6
                                                               .4.2E6
                                                               .3.2E6
                                                               .2.1E6
                                                               .1. 1E6
                                                                O.OEO
                                                                   Tim
1003
 aol
 60:
 40:
 20:
  o:
             16i57 17:23
18:33  19:06
                                                                                                -5.7E6
                                                                                                -4.5X6
                                                                                                '.3.4X6
                                                                                                -.2.3X6
                                                                                                -.1.1X6
             17:00
                           18:00
                                         19:00
                                                      20100
                                                                    21:00
                                                                                  22:00
                                                                                                •.O.OEO
                                                                                                    T±m
                                                                                                          24:

-------
                        fl:P973854
Ref, tass   292.9885     Peak top
Height   .97 volts  Span   298 ppi
Systa file naie
Data   file naie
ResoUJtlon
Group nuiber
lonlzatum Nde
Switching
Ref. lasses   292.9825,
 ft  292.9825
 6  363.9816
 C  366.8987
 D  315.9419
 E  317.9389
 F  319.8965
 6  321.8936
 H  327.8847
 I  338.9792
                     J
                     K
                     L
                     I
       1
     El*
 VOLTBGE
388.9781
338.9792
331.9368
333.9338
375.8364
 Channel   I  338.9792     Peak top
 Helgtt   .98 volts  Span   288 ppi
                                                                                244

-------
TLI Project:      43085
Client Sample:   M23-RB
Method 23 PCDD/PCDF Analysis (a)
             Analysis File:   S975844
Client Project:
Sample Matrix:
TLI ID:

Sample Size:
Dry Weight:
GC Column:
S413-004
M23Train
181-55-8ABDE

1.000
n/a
DB-5

Date Received:
Date Extracted:
Date Analyzed:
Dilution Factor:
Blank File:
Analyst:

09/03/97
09/04/97
09/11/97
n/a
S975815
KB

Spike File:
ICal:
ConCal:
% Moisture:
% Lipid:
% Solids:

SPX23704
SF56117
S975839
n/a
n/a
n/a
Anafytes
2,3,7,8-TCDD
1,2,3,7,8-PeCDD
1,2,3,4,7,8-HxCDD
1,2,3,6,7,8-HxCDD
1,2,3,7,8,9-HxCDD
1,2,3,4,6.7,8-HpCDD
1,2,3,4,6,7,8,9-OCDD
2,3,7,8-TCDF
1,2,3,7,8-PeCDF
2,3,4,7,8-PeCDF
1,2,3.4,7,8-HxCDF
1,2,3,6,7,8-HxCDF
2,3,4,6,7,8-HxCDF
1,2,3,7,8,9-HxCDF
1,2,3,4,6,7,8-HpCDF
1,2,3,4,7,8,9-HpCDF
1,2,3,4,6,7,8,9-OCDF
Totals >^."^-.^
Total TCDD
Total PeCDD
Total HxCDD
Total HpCDD
Total TCDF
Total PeCDF
Total HxCDF
Total HpCDF
Amt (ng}
ND
ND
ND
0.006
0.007
0.03
0.05
ND
ND
EMPC
0.03
0.01
0.01
ND
0.05
EMPC
0.05
•W^^^'-Aiicrt:. (ng)
EMPC
EMPC
0.01
0.04
ND
0.007
0.07
0.07
V 0t EMPO
0.004
0.005
0.005




0.003
0.004
0.005



0.003

0.008

Number DL EMPC
0.007
0.01
2 0.06
2
0.003
1 0.01
5 0.08
3 0.08
ffcrtfo HT Flag*



1.08 29:11
1.41 29:28 	
1.10 32:04 B_
0.91 34:42 B_

	

1.27 28:20
1.38 28:27 	
1.38 28:57 	

1.13 31:12 iZ
	
0.86 34:49 B_
Flags



—



	
                                         Page 1 of 2
                            X237.PSR vZOO. LARS 6.IO.O
 Triangle Laboratories, Inc.®
 801 Capitola Drive • Durham, North Carolina 27713
 Phone: (919) 544-5729 • Fax: (919) 544-5491
                        Printed: 15:34 09/1 «9:
                                                                                    24

-------
TLI Project:      43085
Client Sample:   M23-RB
Method 23 PCDD/PCDF Analysis (a)
             Analysis File:   S975844
IntemaVStandards
3C,:-2,3,7,8-TCDF
13C,2-2,3,7,8-TCDD
13C,:-l,2,3,7,8-PeCDF
3C,2-l,2,3,7,8-PeCDD
13C,2-l,2,3,6,7,8-HxCDF
l3C,:-l,2,3,6,7,8-HxCDD
13Cp-l,2,3,4,6,7,8-HpCDF
13C,2-l,2,3,4,6,7,8-HpCDD
13Cp-l,2,3,4,6,7,8,9-OCDD

Surrogate Standards (Type A)
37CL-2,3,7,8-TCDD
13Cp_-2,3,4J,8-PeCDF
13Cp-l,2,3,4,7,8-HxCDF
l3C,2-l,2,3,4,7,8-HxCDD
13CP_-l,2,3,4,7,8,9-HpCDF
Alternate Standards (Type A)
13CP-l,2,3,7,8,9-HxCDF
13C,2-2,3,4,6,7,8-HxCDF
Recovery Standards -:v: :
13C12-1,2,3,4-TCDD
13C,2-l,2,3,7,8,9-HxCDD
Amt {ng)
2.7
2.5
2.7
2.8
3.0
2.8
2.4
2.7
4.8

\AmMng) W
4.2
3.8
3.6
3.5
3.9
Arrit {ng)
3.0
3.2
r;!":n


%R«s0v*y
68.5
61.5
67.5
69.2
75.6
69.2
60.9
66.8
60.2

fefmiovetf
105
95.0
89.0
87.7
97.8
..% Recovery
75.8
79.3



QC Limits
40%- 130%
40%-130%
40%- 130%
40%- 130%
40%- 130%
40%- 1 30%
25%- 130%
25%- 130%
25%- 130%

•QC Limits
70%- 140%
70%-140%
70%- 140%
70%-140%
70%- 140%
QC Limits
40%- 130%
40%- 130%



Ratio
0.75
0.80
1.52
1.54
0.47
1.23
0.42
1.04
0.86

Ratio

1.45
0.47
1.21
0.42
S-.Rati<£|
0.47
0.47
Ratio
0.81
1.20
m
20:18
21:08
24:39
25:48
28:25
29:10
31:11
32:04
34:42

*}- '#r:
21:09
25:26
28:19
29:05
32:25
ftfcif/r
29:40
28:57
«T
20:55
29:27
Flags



	






; Flags?;;:-




—
^.#ags-v

—
Flags •;.


                      Data Reviewer
                                         Page 2 of 2
              09/18/97
                            X237.PSR T2.00. LARS 6.10.04
 Triangle Laboratories, Inc.®
 801 Cap'rtola Drive • Durham, North Carolina 27713
 Phone: (919) 544-5729 • Fax: (919) 544-5491
                        Printed: 15:3409/18/97-
                                      246

-------
                       Initial
                                    ..Date..
Data Review By:
                                              Calculated Noise  Area:
                                                                       1.68
The Total Area for  each peak with an ion abundance ratio outside
ratio limits has  been  recalculated according to method requirements.
Page No.
09/18/97
Listing of S975844B.dbf
Hatched GC Peaks / Ratio
/ Ret.  Time
Compound/
M_Z.... QC.Log Omit Why ..RT.  OK Ratio  Total.Area... Area.Peak. 1. .  Area.Peak.2..  Rel.RT Compound.Name..  ID.
TCDF
304-306
 304-306

 13C12-TCDF
 316-318
 316-318
 TCDD
 320-322
  320-322

  37C1-TCDD
  328
  328
DC
DC
DC
DC
DC
DC
DC


DC
DC


DC


DC
DC
DC
DC
DC
DC

DC
DC
DC
DC
DC
DC
DC
DC
DC
NL
SN
SN
SN
SN
SN
SN
0

NL
WL


WH
2

NL
SN
SN
SN
SN
SN

SN
SN
SN
SN
SN
SN
SN
SN
WH
0.65-0.89
0:00 RO 0.20
17:33 RO 0.44
13:14 RO 0.38
20:20 0.69
20:55 RO 0.45
21:
21:
45 RO
56 RO
3 .
0.
95
29
Peaks

0:
19:
19:
20:
21:

00
06
50
18
0.




50 RO
65-
0.
0.
0.
0.
1.
0.89
66
74
77
75
43
Peaks
__._ *!

0:
18:
13

:00
:19
:29
18:38
18
19
20
20
20
21
21
21
21
22
22
22
:49
:52
:18
:32
:44
:00
:27
:39
:49
:00
:19
:41
0.
RO
RO
RO
RO

RO
RO
RO
RO

RO
RO
RO
RO
RO
RO
65-0.89
0
0
0
1
0
1
2
0
1
0
1
0
1
0
.55
.44
.96
.51
.80
.70
.56
.49
.06
.71
.13
.90
.27
.28
0.18
1
.52
1 Peak
DC
NL
0:00
19:33
21:09
2 Peaks
                                                0.67
                                                1.54
                                                2.53
                                                8.37
                                                6.71
                                                1.01
                                                1.61
                                                0.00
                                                2.03
                                               15.71
                                               17.76
                                            5,083.04
                                                9.52
                                            5,100.80
                                     7.74
                                 2,182.80
                                                     .818-1.101
                                                        0.000
                                                        0.865
                                                        0.898
                                                        1.002 2378-TCDF       AN
                                                        1.030
                                                        1.071
                                                        1.080
                            0.951-1.049
                                0.000
                                0.941
                         10.02  0.977
                      2,900.24  1.000  13C12-2378-TCDF ISO
                                1.076
                                       Above: TCDF / TCDD Follows
                                                0.78
                                                1.26
                                                1.59
                                                2.99
                                                2.64
                                                1.24
                                                8.04
                                                0.90
                                                0.85
                                                3.14
                                                0.53
                                                0.89
                                                1.59
                                                0.64
                                                 0.69
                                                 0.96
                                                 8.04
                         0.13
                        16.53
                     3,253.66
                     3,270.19
                                     11.63
                                                              16.53
                                                           3,253.66
                            0.851-1.058
                                0.000
                                0.867
                                0.875
                                0.882
                                0.890
                                0.940
                          4.54  0.961
                                0.972
                                0.981
                                0.994
                                1.015
                                1.024
                                1.032
                                1.041
                                1.056
                                1.073
                             0.906-1.094
                                 0.000
                                 0.925
                                 1.001 37C1-TCDD
                                                                                                        SUR1
 Triangle Laboratories, Inc.®  Analytical Services Division
 801 Capitola Drive • Durham, North Carolina 27713
 Phone: (919) 544-5729 • Fax: (919) 544-5491
                                                                        Printed: 15:3409/18/97,

-------
Page  No.
09/18/97
Listing  of S975844B.db£
Matched  GC Peaks / Ratio / Ret. Tin
Compound/
M_Z.... QC-Log Omit Why  . .RT. OK Ratio Total.Area... Area.Peak.1. . Area.Peak.2..  Rel.RT Compound.Name.. ID.. Flags.
13C12-TCDD
332-334
332-334
PeCDF
340-342















340-342
13C12-PeCDF
352-354




N
352-354
PeCDD
356-358




K





DC
0.65-0.89
NL 0:00 RO 8.97 0.53
20:55 0.81 5,629.73 2,525.03
21:08 0.80 3,690.72 1,638.66
21:31 RO 0.91 50.46 26.02
21:39 RO 4.09 5.06 11.71
4 Peaks . 9,375.97
1.32-1.78
DC
DC
DC
DC
DC

DC
DC
DC
DC
DC

DC
DC
DC
DC


DC







DC
DC
DC
DC


DC
DC
DC
DC
DC
NL
Sit
SN
SN
SN

SN
SN
SN
SN
SN

SN
SN
SN
SN
2

NL





5

NL
SN
SN
SN


SN
SN
SN
SN
WH
0:
22:
00
32
23:09
23:
23:
23:
24:
24:
24:
24:
25:
25:
25:
25:
26:
26:
21
32
45
07
27
51
59
08
26
39
48
02
25
RO
RO
RO
RO
RO

RO
RO
RO
RO
RO
RO
RO
RO
RO

0.
1.
0.
0.
3 .
1.
1.
1.
0.
0.
0.
1 .
1.
0.
0.
1.
23
23
36
47
36
32
15
08
52
67
37
27
29
28
57
61
Peaks


0:00
23:
24:
24:
24
25
:45
:16
:39
:58
:26
1.
RO

RO

RO

i 1 V»WL>
0.
2.
0.
0.
0.
7.
1.
0.
0.
1.
0.
5.
4.
0.

05
93
15
28
71
91 4.50
04
89
81
73
31
71 3.47
29
16
0.44
3.
13.
.81
.62
32-1.78
0
1
2
1
2
1
Peaks

0
23
23
24
24
25
25
25
25
26
26

:00
:47
-.54
:27
:40
:00
:26
-.36
:59
:16
:36
1 .
RO
RO
RO
RO
RO
RO
RO
RO
RO
RO
RO
32
6
0
1
0
4
1
4
0
3
0
1
.33
.55
.05
.52
.09
.45

-1.78
.00
. 97
.31
.74
.04
.85
.92
.15
.93
.46
.20
0
27
.07
.12 16.47
10.63 8.53
4,306
14
3,966
.40 2,594.81
.89 12.18
.39 2,345.63
0.906-1.094
0.000
3,104.70 0.990 13C12-1234-TCDD RSI
2,052.06 1.000 13C12-2378-TCDD IS1
28.51 1.018
2.86 1.024
0.905-1.077
0.
0.
0.
0.
0.
3.41 0.
0.
0.
1.
1.
1.
2.73 1.
1.
1.
1.
000
914
939
947
955
963
978
992
008
014
020
032 23478-PeCDF AN
041
047
056
1.072


0.838-1.162
0.
10.65 0
4.17 0
1,711.59 1
5.84 1
1,620.76 1
.000
.963
.984
.000 13C12-PeCDF 123 IS2
.013
.032 13C12-P6CDF 234 SUR2
8,325.43
! PeCDF / PeCDD Follows --
0
0
3
0
6
3
2
.10
.51
.22
.46
.63 10.51
.93 2.85
.30
0.10
0
1
.71
.17
2.39
0.919
0
0
0
0
2.60 0
1.54 0
0
0
1
1
1
-1.025
. 000
.922
.926
.948
.956
.969
.986
.992
.007
.018
.031
 Triangle Laboratories, Inc.® Analytical Services Division
 801 Cap'rtola Drive • Durham, North Carolina 27713
 Phone: (919) 544-5729 • Fax: (919) 544-5491
                                                                    Printed: 15:34 09/1

-------
Page No.
09/18/97
Listing of S975844B.dbf
Matched GC Peaks  / Ratio /  Ret. Tim*
Compound/

M_Z	 QC.Log Omit Why ..RT. OK Ratio Total.Area... Area.Peak. 1.. Area.Peak.2..  Rel.RT Conpound.
                                                                                                   Flags.
356-358
                    2 Peaks
                                           10.56
13C12-P6CDD
368-370


368-370
HxCDF
374-376
















DC




DC


DC
DC
DC


DC
DC

DC
DC
DC
DC
DC

NL


2

NL


SN
SN
SN


SN
SN

SN
SN
SN
SN
SN

0:
25:
25:

00
48
56
1.
RO


32-
5.
1.
1.
Peaks

0:
27:
27:
27:
27:
28:
28:
28:
28:
28:
28:
29:
29:
29:

00
20
29
47
56
12
20
27
33
46
57
05
11
25
29:30
29:41
29:46



374-376
13C12-HXCDF
384-386







384-386
HXCDD
390-392



K
DC
DC
DC


DC
DC



DC

DC


DC
DC
DC


WH
WH
WH
6

NL
SN



SN

SN
4

NL
SN
SN


29:
:54
30:07
30:10
1.




RO
RO


RO


RO
RO

RO
RO
RO
RO
RO
RO
1.78
78
54
50

05-1.43
1.
1.
1.
1.
0.
1.
1.
1.
1.
1.
1.
1.
21
42
12
13
61
55
27
38
45
43
38
86
0.87
1.
,31
0.88
2.
0
0
2
0
.16
.94
.32
.60
.90
Peaks

0
27
28
28
28
29
29
29

:00
:28
:19
:25
:57
:08
:40
:52
0.

RO



RO

RO

0.
2,474.
226.

23
64 1,501.04
54 135.79
0.845-1.155
0.000
973.60 1.000 13C12-PeCDD 123
90.75 1.005


IS3

2.701.18

1.
9.
25.
3.
2.
0.
40.
17.
3.
4.
19.
0.
26
35 5.49
07 13.23
86
11
49
31 22.52
72 10.29
05
82
27 11.17
31
0.61
0.37
0.
1,
5.
0
0
0
117
.42
.39
.94 3.29
.16
.94
.33
.66
.43-0.59
0
0
0
0
0
0
0
0
Peaks

0
27
27
28
28

:00
:52
:59
:20
:25
1
RO

RO
RO
RO
.46
.25
.47
.47
.47
.79
.47
.38

2
6
4,097
4,798
4,659
4
3,871
3
17,426
.05-1.43
0
1
3
1
3
.39
.31
.75
.76
.87
0
3
0
33
4
.43
.69
.03 1.310.17
.83 1,538.50
.59 1.491.21
.14
.01 1,235.48
.46
.46
F / HxCDD Follows —
.47
.37
.09
.02 25.89
.23 7.31
0.955-1.051
0.000
3.86 0.962
11.84 0.967
0.978
0.983
0.992
17.79 0.997 123478-HxCDF
7.43 1.001 123678-HxCDF
1.005
1.012
8.10 1.019 234678-HxCDF
1.023
1.027
1.035
1.038
1.045
3.49 1.048
1.052
1.060
1.062

0.859-1.141
0.000
0.967
2,786.86 0.996 13C12-HXCDF 478
3,260.33 1.000 13C12-HXCDF 678
3,168.38 1.019 13C12-HXCDF 234
1.025
2,635.53 1.044 13C12-HXCDF 789
1.051

0.950-1.014
0.000
0.955
0.959
14.74 0.971
1.89 0.974







AN
AN


AN













SUR3
IS4
ALT 2

ALT1








Triangle Laboratories, Inc.® Analytical Services Division
801 Caprtola Drive • Durham, North Carolina 27713
Phone: (919) 544-5729 • Fax: (919) 544-5491
                                                                  Printed: 15:34 0*18/9:
                                                                                249

-------
Page  No.
09/18/97
Listing of S975844B.dbf
Matched GC Peaks / Ratio / R«t. Time
Compound/'
M_Z....  QC.Log Omit Why ..RT. OK Ratio Total.Area...  Area.Peak.1.. Area.Peak.2..  Rel.RT Compound.Name.
                                                                          ID.. Flags.


M



390-392
13C12-HXCDD
402-404




402-404
28:
DC SN 28:
DC SN 28:
DC SN 28:
DC SN 29:
29:
DC SN 29:
29:
DC WH 29;
5 Pe<

DC NL 0
28
29
29
29
4 Pe.
34 RO
42 RO
46 RO
57 RO
04 RO
11
19
28
40 RO
iks
1.
:00 RO
:33
-.05
:10
:27
aks
1
0
0
2
0
1
. 1
1
2

05
1
1
1
1
1

.56
.77
.39
.91
.45
.08
.37
.41
.80

-1.43
.88
.07
.21
.23
.20
- - ah™
11.
0.
0.
5.
0.
5.
0.
6.
4.
61.

0,
6
3,098
3,631
5,271
12,007
j-o - Uvrrv
80
74
25
26
94
95
64
71
88
71

.74
.76
.27
.09
.85
.97
n / UT^
8.21 5.27

3.09 2.86

3.92 2.79


0.

3.49 3.27
1,695.46 1,402.31
2.004.04 1,627.05
2.875.69 2,396.16

0
0
0
0
0
1
1
1
1

966
0
0
0
1
1

.979
.984
.986
.993
.997 123478-HXCDD
.001 123678-HXCDD
.005
.010 123789-HXCDD
.017

-1.034
.000
.979
.997 13C12-HXCDD 478
.000 13C12-HXCDD 678
.010 13C12-HXCDD 789


AN
AN

AN





SUR4
IS5
RS2

HpCDF
408-410
M


AN

408-410
13C12-HpCDF
418-420


418-420
HpCDD
424-426





424-426
13C12-HpCDD
436-438


436-438

DC NL 0:00
31:12
31:24
31:34
32:25
DC WH 32:55
4 Peaks

DC NL 0:00
31:11
32:25
2 Peaks

DC NL 0:00
DC WL 31:11
31:27
DC SN 31:50
32:04
DC WH 32:25
2 Peaks

DC NL 0:00
DC SN 31:26
32:04
1 Peak
0.88-1.20
RO 3.31
1.13
1.11
1.04
RO 1.28
RO 12.54

0.37-0.51
RO 1.85
0.42
0.42

0.38-1.20
1.13
RO 4.28
1.01
1.19
1.10
RO 2.90

0.88-1.20
RO 1 . 57
RO 1.50
1.04


0.27
57.30 30.40
7.32 3.85
11.64 5.93
6.69 4.19
0.27
82.95

0.58
2,847.33 847.48
2,146.99 632.30
4,994.32
: HpCDF / HpCDD Follows —
0.17
5.90
10.33 5.20
1.18
19.26 10.10
5.22
29.59

1.00
4.61
2,870.60 1.462.22
2,870.60
0.994-1.044
0.000
26.90 1.001 1234678-HpCDF
3.47 1.007
5.71 1.012
3.28 1.040 1234789-HpCDF
1.056

0.936-1. 128
0.000
1,999.85 1.000 13C12-HpCDF 678
1,514.69 1.040 13C12-HpCDF 789

0.976-1.005
0.000
0.972
5.13 0.981
0.993
9.16 1.000 1234678-HpCDD
1.011

0.969-1.031
0.000
0.980
1,408.38 1.000 13C12-HpCDD 678



AN


AN




1 36
SUR5






AN





IS7

 'riangle Laboratories, Inc.®  Analytical Services Division
 101 Cap'rtola Drive • Durham, North Carolina 27713
 >hone: (919) 544-5729 • Fax: (919) 544-5491
                                                                    Printed: 15:3409/1

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Page No.
09/18/97
Listing of S975844B.dbf
Matched GC Peaks / Ratio /  Ret. Time
Compound/
M_Z	QC.Log Omit Why ..RT.  OK Ratio Total.Area... Area.Peak.1..  Area.Peak.2..  Rel.RT Compound.Name..  if..  Flags.
OCDF
442-444
 442-444
 OCDD
 458-460
         AN
 458-460
0.76-1.02
IX
DC
DC
DC
DC
DC
DC
DC
DC
DC
DC
DC
DC
DC
DC

DC
DC
DC


DC
DC

DC

NL
SN
SN
SN
SN
SN
SN
SN
SN
SN
SN
SN
SN
SN
SN

SN
SN
SN
1

NL
SN

SN
1
0:
30:
31:
31:
32:
32:
32:
32:
33:
33:
33:
33:
34:
00
46
07
26
20
27
33
47
00
21
41
54
02
34:21
34:
34
35
35
35
:29
:49
:OS
:26
:56
RO
RO

RO
RO
RO
RO
RO
RO

RO
RO
RO
RO
RO

RO
RO
RO
0.
2.
1.
6.
1.
0.
1.
0.
0.
0.
0.
0.
15.
4.
0.
0
50
46
00
90
05
18
35
22
61
94
34
34
25
.00
.15
.86
1.18
0
1
.20
.58
Peak

0

:00
34:36
34
34
:42
:55
0,

RO

RO
.76-1.02
1
1
0
1
.00
.21
.91
.81
Peak
                                                   / Oeta-CDD and CDF Follows
                                                0.08
                                                0.25
                                                0.42
                                                0.19
                                                0.83
                                                0.28
                                                0.32
                                                0.04
                                                0.76
                                                0.35
                                                0.59
                                                0.81
                                                0.08
                                                0.21
                                                0.57
                                               29.62
                                                0.64
                                                0.21
                                                0.59
                                               29.62
                        0.10
                        3.16
                       22.10
                        0.79
                       22.10
                                    13.73
                                                             10.50
           0.885-1.115
               0.000
               0.887
               0.897
               0.906
               0.932
               0.935
               0.938
               0.945
               0.951
               0.961
               0.971
               0.977
               0.981
               0.990
               0.994
         15.39 1.003  OCDF
               1.011
                1.021
                1.036
            0.885-1.115
                0.000
                0.997
         11.60  1.000 OCDD
                1.006
                                                                               AN
  13C12-OCDD                     0.76-1.02
  470-472         DC  NL   0:00 RO  1.25          0.15
                         34:42     0.86      3,294.68
  470-472               1 Peak                3,294.68
                                  1,523.49
                                                1,
                                                      0.994-1.004
                                                          0.000
                                                  771.19   1.000  13C12-OCDD
                                                                                IS8
  Column Description.
         "Why"  Code  Description	  QC Log Desc.
  M_Z    -Nominal  Ion Mass(es)
  ..RT.  -Retention Time  (mm:ss)
  Rat.l  -Ratio  of M/M+2  Ions
  OK    -RO=Ratio outside Limits
  Rel.RT-Relative Retention Time
      End of Report
         WL-Below Retention Time Window
         WH-Above Retention Time Window
         SN-Below Signal  to Noise Level
         
-------
 il*,3975844 #1-848 Acqtll-SXP-1997 21>43i34 XI+ Voltay* SI* 70S Hoif»:144
 03.9016 r>2 BSUB(256,30,-3.0) PKD(9,5,5,0.05\,S76.0,1.00\,T,T) SxptftCOS
TRIANGLE LABS  Tmxt:M23-*3 TLH43085                         XK7. TIM* -   21>46
       17': 00           18:00            19:00           20', 00           21:00           22:00
rila,S975844  tl-848 Aoqill-SEP-1997 21t43:34  EI+ Voltage SIS 70S Nolfet729
 05.8987 Tt2  SSUB(256,30,-}.0) PJO>(9, 5,5,0.05\,2916.0,1.00\,r,T) EipsEPCUS
TRIANGLE LABS  Tejct:H23-RB TLH43085                         I2C7. TIKE -    21:46
        17:00            18>00           19:00           20:00
F±le:S975844  tl-848 Aojsll-SEP-1997 21,43,34 EI+ Voltage SIR 70S Nbiae,407
315.9419 F:2  BSUB(256, 30,-3. 0) PJCD(9,S,Sr 0.05\,1629. 0,1. 00%,T, T) ExpiEPCUS
TRIANGLE LABS  Te*tsH23-RB 3IHMJ085                        ISJ. TIME -   21:46
 1001
  aol
  eol
  40:
  20:
   o.
                                                            A2.18E7
I V.
        17:00           18:00           19:00           20:00           21:00
 rilesS975844 tl-848 Acqsll-SEP-1997 21,43,34 EI+ Voltage  SIR 70S Hoi.ae-.611
 317.9389 F:2 BSUB(256,30, -3. 0)  P1O>(9,S,5, 0. 05\,2444. 0,1. 00%,F,T) ExptEPCUS
 TRIANGLE LABS  Text,M23~RB  TLI#43085                         IKT. TIME -   21:46
 100S                                                       A2.90E7

  80:

  60:

  40:

  20':

   0.
                                                                                        22,00
        16,59
                   17:40 18:02
       17:00           18:00            19:00           20,00           21:00
File:S975844 #1-848  Acij:ll-S£P-1997 21:43:34  EI+  Voltage SIR 70S
330.9792 F:2 ExpiEPCUS
TRIANGLE LABS   Teit,M23-RB TLI443005                         HKT. TIME -
1003

 80:

 60:

 401

 20:

   0:
                                                                                         22:00
       17:00            181-00           19:00           20:00           21,00
rile,S975844  #1-848 Acq:11-SEP-1997  21:43,34 EI+ Voltage SIR 70S
375.8364  F:2  ExpiEPCUS
TRIANGLE  LABS  Tejct,M23-SS TLI#43085                        UTJ.  TIME -   21:45
1001
                                                                                         '22\00
   80:

   60:

   40:
                                                                           21:08
                                                                       201 S3
                                                                                   21:42

                                                                                21:301
                                                                                            22.11
                                            0X0
                                             Time
                                                                                                       4.9E6

                                                                                                       3.9E6

                                                                                                       2.9E6

                                                                                                       1.9E6

                                                                                                       9.7E5

                                                                                                       .o.oso
                                                                                                          Time



                                                                                                       .6.5E6

                                                                                                       .5.2E6

                                                                                                       .3.9E6

                                                                                                       .2.6E6

                                                                                                       .1. 3E6
                                          O.OEO
                                             Time
                                          6.2E6

                                          5.0E6

                                          3.7E6

                                         .2.5E6

                                         .1.2E6
                                          O.OEO
                                             Tin
                                                                                                   ^U-ft.
        17:00
                         18:00
                                         19:00
                                                         20:00
                                                                         21:00
                                                                                         22:00
                                         -9.8E3

                                         .7.8E3

                                         -5.9E3

                                         -3.9E3

                                          .2.0E3

                                          .O.OEO
                                              Tim
                                                                                                        252

-------
 •il»:S975844 41-848 Acqsll-SXP-1997 21s43s34 SI+ Voltage SIM 70S Holmes 172	
 19.0965 Tt2 BSUB(256,30,-3.0) PXD(7,5,3,0.05\,68».0,1.00\,T,T) ExpsEPCUS
TRIANGLE LABS  TextsM23-RB  TLH43085                        JJW. TIHX -   21t46
                                             A1.16E5
                     19:00              20': 00               21:00
rile:S97S844 tl-848 Aojtll-SXP-1997 21:43:34 EI+ Voltage SIX 70S Noif»s310
321.8936 Ts2 BSUS(256,30,-3.0)  PKD(7,5,3,0.05\,1240.0,1.00\,r,T> XxptXPCOS
TRIANGLE LABS  TextsM23-XB  TLH43085                        INJ. TIME -   21s 46
1004                                         A4.  4X4
                     19:00               20:00               21:00
rilesS975844 tl-848 Acqsll-SXP-1997 21:43:34 EI+ Voltage SIR 70S Noiae:1347
331.9368 F:2 BSUB(2S6,30, -3. 0)  PXD(7,5,3, 0. 05\,5388. 0,1.00%,T,T) ExpsEPCUS
TRIANGLE LABS  TextsM23-RS TLH43085                        IHJ-.
100\                                                     A2.
                                                                                                -2.2X4
                                                                                22:00
                                                                                22» 00
  80:
  60:
  40:
  20:
   o:
                                                             Ul . S4E7
                                          ~r
                     19:00               20:00              21:00
Tile:S975844  tl-848 Acqsll-SEP-1997 21:43:34 EH- Voltage SIR  70S Noiaesl49
333.9338 T:2  BSUB(256,30,-3.0) PKD(7,5,3,0.05\,596.0,1.00\,r,T) ExpsEPCUS
TRIANGLE LABS  TextsM23-RB TLI#43085                        UKT. TIME -   21:46
100$                                                    A3.10E7
                                                                                22:00
  80:

  60:

  40:

  20:
   0.
                                                               2.0517
                     19:00               20:00              21:00
 rile:S975844 41-848 Acqsll-SEP-1997 21:43:34 EI+ Voltage SIR 70S Noiaes64
 327.8847 F:2 BSUB(256, 30, -3 . 0) PKD(7,5,3, 0. 05\,256. 0, 1. 00\,T, T)  ExpsEPCUS
 TRIANGLE LABS  TextsM23-RB TLIt43085                         INJT.  TIME -   21s46
 1003

  80:

  60:

  40:

  20:

   o.
                                                                                22s00'
                       rr
                                           rr
                     19:00               20:00               21:00
 rilesS975S44 «l-848 Acqsll-SEP-1997 21:43:34 EI+  Voltage SIR 70S
 330.9792 Ts2 ExpsEPCUS
 TRIANGLE LABS  TextsM23-RB TLIt43085                         XKT. TIME -   21:45

                                    19:44     30117
                                                                                22:00
  60:
  40:
  20:
   o:
                      19:00'
20:00'
                                                             21:00
                                                                                 22:00'
                                                                                                     Time
                                                                                                 \
                                                           \xo
                                                            Time
                                                                                                 _ J . 7S5
                                                         O.OEO
                                                            Time
                                                        .7.5E6

                                                        -.6.0E6

                                                        -4.5E6

                                                        .3.OE6

                                                        .1. 5E6
                                                         O.OEO
                                                            Time
                                                                                                 -8.1E6

                                                                                                 .6.4E6

                                                                                                 .4.8X6

                                                                                                 .3.2E6

                                                                                                 .1. 6E6
                                                        tO.OEO
                                                            Time
                                                        -6.2E6

                                                        _5.or5

                                                        .3. 7X6

                                                        .2.5X6

                                                        .1.2X6
O.OEO
   Tim
                                                                                                        253

-------
 ll»tS975844 41-848 Aoqill-SST-1997  21:43:34  EH- Voltage SIR 70S Wbi*e:17
 39.8597 r>2 BSOt(256,30,-3.0) PXD(7,5,3t0.05\,68.0,1.00\,rrT) XxptXPCOB
TRIANGLE LABS  T*xt:K23-RB XLH43085                        XKT. TIME -   21:46
 001
                23:00                24:00                25:00
Tile:S975844 #1-848 Acqsll-SEP-1997 21:43:34 ZJ+ Voltage SJJJ 705 Mbi««:63
 41.8567 Ti2 BSUB(256,30,-3.0)  PKD(7,5,3,0.05\,252.0,1.00\,f,T) XzpiXfCUS
TRIANGLE LABS   Text:M23-RB TLIt43085                        IKJ. TIME  -   21:46
1004                          A3.41*4     A1.93E4

 80:
                                                                               26:00
                23:00                24:00                25:00
File:S975844  #1-848  Acg:ll-SJEP-1997 21:43:34 EI+ Voltage SIX  705  No±ae:21
351.9000  T:2  BSUB(256,30,-3.0) PXD(7,5,3r0.05\,84.0,1.00\,r,T)  SxpsEPCUS
TRIANGLE  LABS  Text: M23-X.B TLI#43085                        ItU.  TIME -
                                                                               26:00
                                                                            21:46
 1001
  80:
  60:
  40:
  20:
                                                                 A2.35E7
                                                                    ,
                23:00                24:00                 25:00                 26:00
 rile:S$75fl44 #1-848 Acq:ll-SEP-1997 21:43:34  EI+ Voltage SIR 70S Noiae:60
 353.8970 r-.2 BSUB(256,30,-3.0) PKD(7, 5,3, 0. 05\,240. 0,1. 00\,T, T) Exp:EPCUS
 TRIANGLE LABS  T&xt:M23-RB TLIJ43085                         IJKT. TIME -   21:46
 1003

  80J


  40J

  20J

   0.
                                                                  Al.62Z7
                23i00                24:00                25:00
FiletS975844 fl-848 Acq:ll-SEP-1997 21:43:34 EI+ Voltage SIR  70S
330.9792 Ts2 Eip:EPCUS
TRIANGLE LABS   Text:M23-RB  TLI#43085                        IKJ. TIME -
1004
                                  23:51 24:08
  80:
  60:
  40:
  20:
   o.
                                                                                26:00
                                                                            21:46
                  ~r
                                        -r
                23:00                24:00
File:S975844  #1-848  Acqsll-SEP-1997 21:43:34 EI+ Voltage SIR 70S
409.7974 T:2  ExptEPCUS
TRIANGLE LABS  Text:M23-JlB HJ#430«5                         HKT. TIME -
1001
                                                                                26:00
                                                                             21:46
                 23:00
                                      24:00
                                                           25:00
                                                                                26: 00
 8.0E6

 6.4E6

 4.8E6

 3.2E6

.1. 6E6
                                                                                                      O.OEO
                                                                                                         Tiae
 5.4E6

 4.3E6

 .3. 2E6

 .2.2E6

 .1.1E6
 O.OEO
    Time
 7.4E6

 S.9E6

 4.4E6

 2.9E6

 1. 5E6

 .O.OEO
    Tim
23
22:36 23: OS
I I 23:30
_JL__L_J_
45

^A_ - - ^ilL2£i°JL_

26:10
25:59 1
25:34 I 1 i
-^jiL^LiAL
26:39

1
                                                                                                     -8.2E3


                                                                                                      4.9X3

                                                                                                      3.3X3

                                                                                                      1.6X3

                                                                                                      0.0X0
                                                                                                          Tim
                                                                                                           254

-------
TM.e:SS75844 41-848 AcqU.l-SXr-1997 2J.t43l34 XI+ Voltage SIX 70S
355.8546 T>2 BSOB(256,30,-3.0) PKD(7,5,3,0.05\,484.0,1.00\,r,T) XxptXTCOS
TSIANCLX LASS  Text:M23-XB TLH43085                         1X7. 3TME "   21*46
1003

 80.

 so:

 40.

 20:

  o:
          24:00                          25.00                         25:00
F±le:S975844 41-848 Aoqtll-SXP-1997  21:43:34 XI+ Voltage SIX 70S Hoime:22
357.8516 T:2 BSUB(256,30,-3.0) PKD(7, 5,3, 0,05\, 88. 0,1.00\,f,T) ErpiEPCUS
TRIANGLE LABS  TexttM23-RB TLI4430S5                        ZJK7. TIHX  -   21:46
1001                                                                          Al.  4X4
                             A1.05X5
                                                    A4.43X4
      A1.96S4
        A/\A   A5.96E3
     A^/  \/\A»^A^AA»- ^
                                                                                        Al.4524
                                                                              A7.08X3
      I
      ft
y^Jl
.2.7*4






.1.1*4

-5.4JT3
           24 .-00                         25:00
 Tile:S975844 #1-848 Acq:ll-SEP-1997 21:43:34 EI+ Voltage  SIX 70S Koiae:260
 367.8949 T:2 BSUB(256, 30, -3. 0) PKD(7,5,3, 0.05\,1040. 0,1. 00\,r,T) Exp:EPCtJS
 TKIAXGLE LABS  TeitiM23-RB TLI443085                         IJU. TIMX -   21:46
 1004                                                           A1.50.E7
  SO.

  eo:

  40J

  20:
                                                                      1.36X6
           24:00                          25:00                         26:00
 r±letS975844  41-848 Acqsll-SEP-1997  21:43:34 EI+ Voltage SIR 70S NOi»et4S
 369.8919  T:2  BSOB(256,30,-3.0) PXD(7,5,3,0.05\,180.0,1.00\,T,T) Exp:XPCVS
 TSIASGLX  LABS  Text:H23-RB TLH43085                        XMT. TIME  -   21:45
 1001                                                            A9 ?4X6
   80.
   60.
   40.
   20.
                                                                      19.08X5
                                                                        /\
           24:00                         25:00                          2$<00
  File:S975844 41-848 Acq:ll-SEP-1997 21:43:34 EI+ Voltage  SIS 70S
  330.9792 r:2 Xxp:EPCOS
  TRIANGLE LABS  T&Xt:H23-R3 TLH43085                         IKT. TTHE -   21:45
  1001
   so:
   50J

   40.

   20:

    0.
                                                                  25:45
                                                                                  25:17
            .5.0X6

            .4.OE5

            -3.0X6

            -2.0X6

             .9.9X5
                                                                                                    0.0X0
                                                                                                       Time
             .3.2X6


             .2.6X6


             .1. 9X6


             .1. 3X6


             .6.4X5
                                                                                                    .O.OEO
                                                                                                        Time
             .7.3X6

             .5.9X6

             .4.4X6

             '.2.9X6

             .1.5X6
            24:00
                                           25iOO
                                                                         26100
               0.0X0
                  Time\

-------
 11»,S975844 tl-405 Aoqtll-SXP-1997 21t43t34  XI* Voltage SIX 70S Hoime:345
 73.8208 Fi3 3SUB(256,30,-3.0) PXD(7,5,3,0.05\r13aO.Or1.00\rr,T) frptXPCUS
TRIAHSLX LASS  Text,M23-RB TLH43085                         IWT. TIM* -   21>46
   27:12 27,24 27,36  27,48 28,00 28,12 28,24  28:36 28:48 29:00  29:12 29:24 29,36  29:48 30:00 30tl2
 ±19:3975844 tl-405 Actj,ll-3EP-1997 21,43,34 EI+ Voltage SIX 703 Hoist,286
 75.8178 T:3 3SUB(256,30, -3.0)  PKD(7,5,3, 0. 05%, 1144. 0,1. 00\,T,T) XzpiXPCUS
TRIANGLE LAMS  Text:M23-RB TLH430SS                        IXT. TIME -   21:46
                                     Al.78X5
                                         I
 003
 80:

 sol
 40:
 20:
                                     A2.25X5
                    A2.05X4
                                                        A1.12X5
                                                                                  A3.29X4
-7.9X4

.6.3X4

.4.8X4

.3.2X4

-.1.6X4
                                                                                L^^T^"^^"
                                                                                                      0.0X0
                                                                                                         Time
   27:12 27:24  27:36 27:48 28:00  28:12  28:24 28:36 28:48  29:00 29:12 29:24  29:36 29:48 30:00  30:12
 File:S97S844  tl-405 Acq:ll-SXP-1997 21:43:34 EI+ Voltage SIR  70S Soime:380
  83.8639 T:3  BSUB(256,30, -3.0) PKD(7,5,3, 0. 05\,1520. 0,1.00\,T,T) Exp:EPCUS
 TRIANGLE LABS  Text:M23-RB TLIt43085                        INJ. TIHX -    21:46
 1004                                    Al  54X7
                                                                                                         Time
  40:

  20:

   ol
                                                         A1.49E7
                                                                                A1.24E7
                                                                                                    .4.0E6

                                                                                                    13.0X6

                                                                                                    ,2.0X6

                                                                                                    .1. 0X6
                                                                                                     0.0X0
   27:12  27:24 27:36 27:48  28:00  28:12 28:24 28:36  28:48 29:00 29:12  29:24  29:36 29:48  30:00 30:12   Time
 rile:S975S44 tl-405 Ac
-------
fiJLetS97S844 tl-405 Aoq:ll-SEP-1997 21:43:34 XIr Voltage aim  70S HOifetlJV
389.8156 T:3 BSOB(256,30,-3.0) fXD(7,5,3,0.05\,520.0,1.00\,r,T) ElptEPCUS
TSIAXGLX LABS  TexttM23-SB TLI'43085                        UKT. TIMS -
1001                       A2.59ES
80.


60.


40.


20J


 0.
      27:48   28:00   28:12    28:24   28»36   28:48    25:00   25:12   25:24
riletS975844 tl-405 Acqtll-SEP-1997 21:43:34 EH- Voltage SIS 70S Noime:329
391.8127 T:3 BSUB(256,30,-3.0) PXD(7,5,3,0.05\,1316.0,1.00\,F,T) XxptEPCOS
TRIANGLE LABS  TexttM23-SB TLIt43085                        INJ. TIME  -    21:46
1001
                                     A8.21E4
                                                     A6.84E4
                                                                                   A6.11S4
                                       (\              A
                                       /V             /\
                                       ^   ^    -      ^^
                                                              A4.52S4
                                                                          A3
. 92X4    A
 \      A
    -
                                                                                 29:36   29:48
       27:48    28:00   28:12    28:24   28:35   28t48    29:00   23:12   29:24    25:36   29:48
 rile:S97SB44 tl-405 Acqtll-SEP-1997 21:43:34 EI+ Voltage SIS 70S Noiae:312
 401.8558 T:3 BSOB(256,30,-3.0)  PKD(7,5,3,0.OS\,1248.0,1.00\,F,T) ExptEPCOS
 TSIANSLE LABS  Tej[tsM23-SB TLIt430B5                        IKJ. TIME -   21:45
 1001                                                                      A2.88E7
  so:

  50:

  40:

  20:
                                                               A2.00E7
      27:48    28:00   28:12    28:24    28:36   28:48    29:00    29:12   29:24    25:35   29:48
 File:S975844 tl-405 Acqtll-SEP-1997  21:43:34 IX* Voltage SIS 70S Noiaetl67
 403.8529 F:3 BSOB(256,30,-3.0) PKD(7,5,3,0.05\,668.0,1.00\,r,T) ExptEPCOS
 TSIANSLE LABS  TexttM23-SB  TLIt43085                        IVJ. TIME -   21:46
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 392.9760 Ts3 XxptEPCOS
 TRIANGLE LABS  TextiM23-SB TLIt4308S                         IJKT. TIME -   21:45
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-------
 ile>3975844  #1-430 Aoqill-SXP-1997 21i43i34 XI* Voltao* SI*  70S Hoif9:215
 07.7818 Ti4  BSVB(256,30,-3.0) PKD(7,5,3,0,05\,860.0,1.00\,T,T) XxpiXTCDS
 •IAKSLX LASS  TexttM23-XB TLH43085                        HKT. TZKK  -   21:46
 31-00     31,12      31,24     31,36     31,48     32,00      32,12     32,24
 il»:S975844  H-430 Aajtll-SEP-1997 21,43,34 SI+ Volt*?* SIS 70S Halfe,64
 09.7789 T,4  BSOB(256,30,-3.0) PKD(7,5,3,0.OS\,256.0,1.00\,T,T)  XxptXPCOS
TRIANGLE LABS  Text:H23-XB TLH43085                         ItKT. TIMS -   21,46
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  31-00     31:12     31:24     31:36      31,48     32,00     32:12     32:24
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 17.8253 T:4 BSOB(256,30,-3.0)  PKD(7,5,3,0.05\,1476.0,1.00*,T,T) Exp-.EPCUS
TRIANGLE LABS  Teit:M23-XB  TLH43085                        IKT. TIME "   21:46
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 003
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          A3.2315
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                                                                                   32,36
                                                                                              32:48
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                            A5.71E4
                                                                        A3.81E4
                                                                                    A9.02E3
                                                                                    32:36
                                                                                              32:48
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423.7766 T:4 *SUB(256,30, -3 .0) PKD(7,5,3
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435.8169 T:4 BSVB(256,30, -3.0) PKD( 7, 5,3, 0. 05\,1S40. 0,1.00%, f,T) Exp:EPCUS
TRIANGLE LABS Text:M23-RS 1X1*43085
1001
801
601
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437.8140 f:4 BSUB(2S6,30, -3. 0) PKD(7,5,
TRIANGLE LABS Text:M23-RB TLIf43085
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430.9729 F:4 XxpiXPCOS
TRIANGLE LABS Text:M23-RB TLH43085
100
80
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443.7399 T:4 BSUB(356,30,-3 .0) PKD(7,5,3,0.05\,152.0,1.00\,r,T) Exp:EPCUS
TRIANGLE LABS Tuxt:M23-XB TLHH30S5
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901
801
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601
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301

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101
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430.9739 F:4 Exp:EPCUS
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TRIANGLE LABS Text :M23 -JIB TLHH30B5
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459.7348 Fs4  BSUS(256,30,-3.0)  PKD(7,S,3,0.05\,92.0,1.00\,F,T) XxptXPCUS
TRIANGLE LASS  Text:M23-XB TLIf43085                        IKJ. TIMS -   21,46
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 469.7779 F,4 BSU3<256,30,-3.0) PKD(7,5,3,0.05\,204.0,1.00\,F,T) ExptEPCOS
 TRIANGLE LASS  T&It:M23-RB TLH43085                        IKT. TIME -   21:45
 100*                                Al.
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                         34,36        34:42         34:48         34,54
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 471.7750 F:4 BSUB(256,30,-3.0) PXD(7,5,3,0.05\r16B.0,1.00\,F,T) Exp:EPCOS
 TRIANGLE LABS  T&rt:H23-RB  TLI#43085                        IKJ. TIME -   21:46
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Channel    I  338,9792     Peak top
Height  1,51 volts  Span  298 ppi

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Data   file naie         fl=$975843
Resolution                  18686
Group rajtef                    2
Icnlzatlon axte               £1*
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Ref,  lasses   292,9825,   416,9768
fl  293      J   331     S   368
             K   332     T   378
             L   334     U   376
             1   348     V   418
             H   342
             0   352
             P   354
             Q   356
             R   358

  tef, lass   416,9768     Peak top
  Height   ,27 volts Span   288 ppi
262

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09.7789 F:4 Exp:EPCUS
ample Text:M23-RB TLI#43085                         INJ. TIME =
                                                                      35:00
                                                                                         16.0E4
                                                                                         L4.5E4
                                                                                         L3.0E4
                                                                                         L1.5E4
                                                                                         LO.OEO
Time
                                                                  21:46 File Text:M23-RB TLI#43»
UU1
80 j
60J
40J
20J
0 "


&2 69Ep
/I
A
I\J^A^ A3'3^E4 A A* . ^^^^^ *
L1.2E5
L9.0E4
L6.0E4
L3.0E4
- O.OEO
31 loo 	 32100' ' ' 33 100 34 100 35loO Time
Lle:S975844 #1-430 Acq:ll-SEP-1997  21:43:34 EI+ Voltage SIR 70S
L7.8253 F:4 ExprEPCUS
ample Text:M23-RB TLI#43085                         INJ.  TIME =
                                                                  21:46 File Text:M23-RB TLI#43»
                                                                                        _1.9E6
JU2
80J
50J
10 j
20 j
0 "
jj.jj.j-
J
32:25
II A
A
\
IV / V
L1.5E6
L1.1E6
L7.4E5
L3.7E5
1 O.OEO
31 100 	 32 100 	 33 loo' 34? 00 35100 Time

-------
                                                                                                   00
ile:S975844 #1-430 Acq:ll-SEP-1997  21:43:34  EI+ Voltage  SIR  70S
57.7377 F:4 Exp:EPCUS
ample Text:M23-RB TLI#43085                      ._  INJ.  TIME =
00%                                          ,  A1.05E5 )
                                                                 21:46 File Text:M23-RB TLI#43»
                                                                                       ^1.6E4
 33:00                        34100                       35:00
Lle:S975844 #1-430 Acq:ll-SEP-1997 21:43:34 EI+ Voltage SIR 70S
59.7348 F:4 Exp:EPCUS
•unple Text:M23-RB TLI#43085                       .INJ, TIME =
                                                                                           Time
                                                                 21:46 File Text:M23-RB TLI#43»
                                                                                       r_1.5E4
33:00                        34100                        35iOO
.le:S975844  #1-430 Acq:ll-SEP-1997  21:43:34  EI+  Voltage  SIR 70S
19.7779 F:4  Exp:EPCUS
imple Text:M23-RB TLI#43085                         INJ.  TIME =
                                                                                        O.OEO
                                                                                           Time
                                                                 21:46 File Text:M23-RB TLI#43»
' \SJM
!0_:
;QJ
OJ
OJ
o:



•

J. . U£.O
L8.3E5
L6.2E5
L4.1E5
L2.1E5
n ORD
i • i • i § i i i i 	 1 	 1 	 1 	 1 	 1 	 1 	 1 i 	 •— — • - " "
33:00 34:00 35:00 Time

-------
TLI Project:
Client Sample:
                 43085
                 TLI LCSD
Method 23 PCDD/PCDF Analysis (a)
             Analysis File:   S975832
Client Project:
Sample Matrix:
TLI ID:

Sample Size:
Dry Weight:
GC Column:
S413-004
XAD
TLI LCSD

1.000
n/a
DB-5

Date Received:
Date Extracted:
Date Analyzed:
Dilution Factor:
Blank File:
Analyst:

//
09/04/97
09/11/97
n/a
S975815
BJG

Spike File:
ICal:
ConCal:
% Moisture:
% Lipid:
% Solids:

SPX23704
SF56117
S975814
n/a
n/a
n/a
Anatytes •; -i":'£?%$*$x3:-$i-f>$:.
2,3,7,8-TCDD
,2,3,7,8-PeCDD
,2,3,4,7,8-HxCDD
,2,3,6,7,8-HxCDD
,2,3,7,8,9-HxCDD
,2,3,4,6,7,8-HpCDD
.2,3,4.6,7,8,9-OCDD
2,3,7,8-TCDF
1.2,3,7,8-PeCDF
2,3,4,7,8-PeCDF
1,2,3,4,7,8-HxCDF
1,2.3,6,7,8-HxCDF
2,3,4,6,7,8-HxCDF
1,2,3,7,8,9-HxCDF
1,2,3,4,6,7,8-HpCDF
1,2,3,4,7,8,9-HpCDF
1,2,3,4,6,7,8,9-OCDF
Inftunaf ^innriarrfe ' "^ '••'••••'• --: •'•' ":
.. emai aiarraaras ; ....,,. ,,. :;;|,v .,
l3C,2-2,3,7,8-TCDF
13C12-2,3,7,8-TCDD
3C,2-l,2,3,7,8-PeCDF
[3Cr.-l,2,3J,8-PeCDD
13C12-l,2,3,6,7,8-HxCDF
13C12-l,2,3,6,7,8-HxCDD

13C12-l,i3,4,6,7,8-HpCDF
l3C12-l,2,3,4,6,7,8-HpCDD
13C1;-1,2,3(4,6,7,8,9-OCDD
.A: fAmt»: (ng)
0.36
1.9
1.7
1.8
1.9
1.8
3.6
0.37
1.9
1.9
1 7
1.8
1.7
1.8
1.8
1.6
2.8
..::-.:.• _.. -,.-.• . .-i
.Amt \ng)
2.6
2.4
2.6
2.7
2.9
28

2.5
2.7
4.8
BL 1


*»
% Recover;
65.4
60.9
64.9
66.7
72.8
70 3

62.5
67.1
60.2
SMPO



f QC tpmrts
40%- 130%
40%- 130%
40%- 130%
40%- 130%
40%- 130%
Ar\or, \i.r\ot-

25%- 130%
25%-130%
25%- 130%
B*tf6«:^
0.78
1.64
1.24
1.23
1.24
1.04
0.83
0.82
1.52
1.53
1 TO
i.zy
1.29
1.28
1.32
1.09
1.09
0.88

Ratio
0.76
0.80
1.56
1.48
0.50
1 04
i.ZA
0.42
0.99
0.87
!:v?*r!v-v:
21:1-3
25:51
29:07
29:12
29:29
32:04
34:38
20:23
24:42
25:29
OQ.OO
2.Q.2Z
28:29
28:59
29:42
31:12
32:25
34:43

RT
20:22
21:12
24:42
25:50
28:28
on. i o
Zy.lZ.
31-11
32:04
34:38
^fcg*^
—
—

Ftegs










Triangle Laboratories, Inc.®
801 Capitola Drive • Durham, North Carolina 27713
Phone: (919) 544-5729 • Fax: (919) 544-5491
                                      Page 1 of 2
                                                                       X237.PSR viOO. LARS 6.10.04
                                                                    Printed: 12:0309/18/97
                                                                            269

-------
TLI Project:
Client Sample:
43085
TLI LCSD
     Method 23 PCDD/PCDF Analysis (a)
                   Analysis File:   S975832
 AttertvateStervrfaitts(Typ*A}   Amt (ng)
                        % Rwovary   QC Limits     Ratto
l3C,2-l,2,3,7,8,9-HxCDF
l3C,2-2,3,4,6,7,8-HxCDF
            3.0
            3.1
75.4
77.5
40%-130%
40%-130%
0.51
0.50
29:41
28:59
 Recovery Standards
                                                 Ratio
                                 8T
 13C,2-1,2,3,4-TCDD
 I3C12-l,2,3,7,8,9-HxCDD
                                                  0.80
                                                  1.20
                                20:59
                                29:29
    Data Reviewer
                                           , -L t^,\v^
                    09/18/97
                                             Page 2 of 2
                                                              X237_PSR»ZOO, LARS 6.IOM
  Triangle Laboratories, Inc.®
  801 Caprtola Drive • Durham, North Carolina 27713
  Phone: (919) 544-5729 • Fax: (919) 544-5491
                                                          Printed: 12:03 09/18/9'

-------
                       Initial
                                  ..Date..
Data Review By:
JJTL     ") / (j / !+•  Calculated Noise
                                                            Area: n/a
The Total  Area for each peak with an ion abundance ratio outside
ratio limits has been recalculated according  to method requirements.
Page No.      1
09/18/97

Compound/
M_Z.... QC.Log Omit Why
Listing of S975S32B.dbf
Hatched GC Peaks / Ratio /  Ret. Time
.RT.  OK Ratio Total.Area...  Area.Peak.1..  Area.Peak.2..  Rel.RT Compound.Name.. ID.. Flag*.
TCDF
304-306









304-306
13C12-TCDF
316-318




316-318
TCDD
320-322

















320-322
0.65-0.89
DC
DC
DC
DC
DC
DC
DC

DC
DC


DC
DC
DC

DC


DC
DC
DC
DC
DC
DC
DC
DC
DC
DC
DC
DC
DC

DC
DC
DC
DC
NL
SN
SN
SN
SN
SN
SN

SN
WH
, 1

NL
SN
SN

SN
1

NL
SN
SN
SN
SN
SN
SN
SN
SN
SN
SN
SN
SN

SN
SN
WH
WH
0:00 RO
16:48
18:03
19:
19:
19:
20:
20:
21:
22:
11
30
54
08
23
56
42
RO
1.25
0.86
0.
60
0.70
RO
RO
RO

RO
RO
1.
0.
0.
0.
0.
0.
09
98
27
82
35
18
Peak

0:
19:
19:
20:
20:

00
32
52
22
53
0.
RO



RO
0.14
1.56
2.44
18.
3.
11.
0.
461.
0.
0.
461.
85
19
58
55
06 207.61
64
55
06
65-0.89
15.
0.
0.
0.
1.
Peak

0;
18:
18:
18
19
19
19
19
20
20
20
20
21
21
21

:00
:37
:42
:53
:08
:15
:21
:55
:22
:30
:44
:54
:00
-.13
:48
22:19
0.
RO

RO
RO
RO

RO

RO


RO
RO

RO
RO
22:38 RO
22:40 RO
20
69
77
76 4
14
4
65-0.89
1.
0
12.
2
0
0
0
0
3
0
0
1
2
0
6
0
1
0
.33
.73
.60
.80
.43
.73
.25
.75
.32
.75
.74
.90
.83
.78
.50
.43
.06
.27
1 Peak
0.
6.
18.
,035.
21.
09
32
60
05 1,746.44
35
0.820-1.101
0.000
0.825
0.
0.
0.
0.
0.
253.45 1.
1.
1.

0.951-
0.
0.
0.
2,288.61 1.
1.
886
942
957
977
989
001 2378-TCDF AN
077
115

1.049
000
959
975
000 13C12-2378-TCDF ISO
025
,035.05

0
0
0
0
0
1
0
2
1
1
0
0
0
322
.11
.76
.09
.35
.55
.07
.34
.13
.33
.80
.94
.51
.94
.42 141.35
0.18
0.92
0.55
0.57
0.853-1.059
0
.000
0.878
0
0
0
0
0
0
0
0
0
0
0
181.07 1
1
1
.882
.891
.903
.908
.913
.939
.961
.967
.978
.986
.991
.001 2378-TCDD AN
.028
.053
1.068
1.069
322.42
 Triangle Laboratories, Inc.® Analytical Services Division
 801 Capitola Drive • Durham, North Carolina 27713
 Phone: (919) 544-5729 • Fax: (919) 544-5491
                                                                     Printed: 12:0309/18/97
                                                                                     271

-------
Page No.
09/18/97
Listing of S975832B.db£
Hatched GC Peaks / Ratio / Ret.  Tin
Compound/
M_Z.... QC.Log Omit Why  ..RT. OK Ratio Total.Area...
                          Area.Peak.1.. Area.Peak.2.. Rel.RT Compound.Name..  ID..  Flags.
13C12-TCDD
332-334
DC
DC
DC
NL
SN
SN
0.65-0.89
0:00 RO 24.67 0.16
19:52 RO 1.13 13.47
20:36 RO 2.05 2.35
20:59 0.80 4,680.21 2,079.73
21:12 0.80 3,036.35 1,350.47
21:33 RO

332-334
PeCDF
340-342









340-342
13C12-PeCDF
352-354







352-354
PeCDD
356-358






356-358
13C12-PCCDD
368-370

DC

SN
3
21:46 RO
Peaks
1.12
1.38
42.13 26.58
3.95
0.906-1.094
0.000
0.937
0.972
2,600.48 0.990 13C12-1234-TCDD RSI
1,685.88 1.000 13C12-2378-TCDD IS1
23.80 1.017
1.027
7,758.69
1.32-1.78
DC
DC
DC
DC

DC
DC

DC
DC


DC
DC
DC

DC
DC
DC
DC


DC
DC
DC
DC
DC
DC



DC
DC
NL
SN
SN
SN

SN
SN

SN
SN
2

NL
SN
SN

SN
SN
SN
SN
1

NL
SN
SN
SN
SN
SN

1

NL
SN
0:00
22:36
23:49
24:21
24:42
24: 53
25:01
25:29
26:08
26-27
Peaks

0:00
23:46
24:20
24:42
24:59
25:22
25:28
26:27
Peak

0:00
23:57
24:43
24:52
25:04
25:30
25:51
Peak

0:00
24:43
RO
RO

RO

RO


RO
RO

1.
RO
RO





RO

1.
RO
RO
RO

RO
RO


1
RO
RO
25:50
0.
0.
1.
1.
1.
1.
1.
1.
1.
0.

88
31
33
89
52
11
59
53
02
56

0.
2.
22.
10.
1,810.
10.
27.
1,823.
1.
3.
3,633.

12
07
22
30
32 1,092.57
22
22
25 1,103.61
51
88
57
32-1.78
1.
1.
1.
1 .
1.
1.
1
0

00
15
40
56
.74
.50
.48
.95

0.
11.
12
.53
14.07
3,441.27 2,098.74
14.25
3
29
8
3,441
.32-1.78
0
0
1
1
2
1
1

.32
0
2
1
.86
.09
.97
.38
.08
.91
.64

-1.78
.86
.43
.48
0
0
2
3
2
0
1,165
1,165
.08
.96
.95
.27

.10
.79
.63
.97
.47
.82
.51 724.15
.51
0.907-
0.
0.
0.
0.
717.75 1.
1.
1.
719.64 1.
1.
1.

1.078
000
915
964
986
000 12378-PeCDF
007
013
032 23478-PeCDF
058
071






AN


AN



0.833-1.162
0.000
0.962
0.
1,342.53 1.
1.
1.
985
000 13C12-PeCDF
.011
.027
1.031 13C12-PeCDF
1

.071


123 IS2


234 SUR2


0.921-1.026
0
0
0
0
0
0
441.36 1

.000
.927
.957
.963
.970
.987
.001 12378-PeCDD







AN

0.845-1.155
0.10
2
.22
1,982.60 1,183.63
0
.000

0.957
798.97 1
.000 13C12-P6CDD
123 IS3
 Triangle Laboratories, Inc.®  Analytical Services Division
 801 Caprtola Drive • Durham, North Carolina 27713
 Phone: (919) 544-5729 • Fax: (919) 544-5491
                                                                    Printed: 12:03

-------
  Page No.

  09/18/97
Listing  of S975832B.dbf
Matched  GC Peaks / Ratio / Ret. Time
 Compound/

 M.Z.... oc.Log omit Why . .RT. OK Ratio Total.Area... Area.Peak.1..  Ar.a.P.ak.2.. R.I.RT Compound.*
                                                                                             Ian*.. ID. .Flags
368-370
HXCDF
374-376













374-376
13C12-HXCDF
384-386









384-386
HxCDD
390-392













DC
DC
DC
DC
DC
DC
DC

DC

DC

DC
DC

DC
DC
DC
DC

DC
DC
DC
DC
DC


DC
DC
DC
DC

DC

DC
DC
DC
DC
DC

2
NL
SN
SN
SN
SN
SN
SN

SN

SN

SN
SN
4
NL
SN
SN
SN

SN
SN
SN
SN
SN
3

NL
WL
SN
SN

SN

SN
SN
SN
SN
SN

25:59
Peaks
0:00
27:22
27:30
28:02
28:22
28:29
28:44
28:48
28:59
29:13

29:16

29:24

29:30
29:42
29:54
Peaks
0:00
27:20
27:30
28:28
28:42

28:59
29:13
29:16
29:24
29:41
29:58
30:01
Peaks

0:00
27:44
27:54
28:04

28:23

28:29
28:37
28:42
28:51
28: 58
29:07

1.
RO
RO
RO
RO
RO
RO
RO

RO

RO

RO
RO

0.
RO
RO
RO

RO
RO
RO

RO

1 .
RO
RO
RO
RO

RO

RO
RO
RO
RO
RO

1
.50
.05-1.43
.1.89
1
1
2
1
1
2
1
1
0

1

1

1
1
0

43
0
0
0
0
1

0
0
0
0
0
0
0

05
1
1
0
0

0

2
1
1
3
4
1
.53
.48
.02
.29
.29
.60
.72
.28
.80

.30

.65

.52
.32
.91

-0.59
.55
.29
.39
.50
.50

.50
.64
.32
.74
.51
.55
.60

-1 . 43
.49
.78
.87
.89

.85

.06
.56
.62
.15
.50
.24
180
2,163
*
1
4
10
1
1,561
2,046
2
2
1,541
2

1

1

3
1.479
2
6,629
3
2
9
2,962
2

2,919
3
1
1
2,468
2
3
•79 108.57
.39
D / HxCDF Follows --
.77
.26
.37
.30
•66 878.60
•94 1,154.87
.55
.02
•86 865.45
.67

.59

.90

.23
.08 841.99
.49
.54
.29
.61
.95
•73 982.38
.55

•87 972.79
.70
.27
.31
•56 831.41
.28
.16
72.22 1.
006
•
0.955-1.052
0.000
0.
0.
0.
683.06 0.
892.07 1.
1.
1.
676.41 1.
1 .

1 .

1 .
1.
637.09 1.

0.359-
0.
0.
0.
1,979.85 1.
1 .
1,947.08 1.
1.
1.
1.
1,637.15 1.
1.
1
8,351.16
961
966
985
996 123478-HXCDF
001 123678-HXCDF
009
012
018 234678-HxCDF
026

028

03 3
036
043 123789-HXCDF

1.141
000
960
966
000 13C12-HXCDF 678
008
018 13C12-HXCDF 234
026
028
033
043 13C12-HXCDF 789
053
n*\A
U34



All
AN

AN






AN




IS4

ALT2


ALT1



1
1
1
0

3

2
5
1
0
0
985
.32
.52
.61
.90

.09

.31
.64
.88
.60
.94
•19 544.61
0.950-1.015
0. nnn
0.
0.

0 .

0 .
0.
0.
0.
0.
0.
440.58 0.
950
955

961

972
975
980
983
988
992
QQ7 1 *>T4"7Q_Ui,/~™r\












                                                                                         -HxCDD
                                                                                                   AN
Triangle Laboratories, Inc.® Analytical Services Division
801 Caprtola Drive • Durham, North Carolina 27713
Phone: (919) 544-5729 • Fax: (919) 544-5491
                                                                  Printed: 12:03

-------
Page No.     4
09/18/97


Compound/

M_Z.... QC.Log Omit Why
Listing of S975832B.db£
Matched GC Peaks / Ratio / Ret. Time
.RT.  OK Ratio Total.Area...  Area.Peak.1..  Area.Peak.2.. Rel.RT Compound.Name. .  ID.. Flags.





390-392
13C12-HXCDD
402-404





402-404
HpCDF
408-410



408-410
13C12-HpCDF
418-420





418-420

HpCDD
424-426


424-426
13C12-HPCDD
436-438



436-438
29:12
29:29
DC SN 29:37 RO
DC WH 29:43 RO
DC WH 29:53 RO
3 Peaks
l.i
DC NL 0:00 RO
DC WL 27:54 RO
DC SN 28:34
29:12
29:29
DC SN 29:42 RO
2 Peaks
0.
DC NL 0:00 RO
31:12
DC SN 31:32 RO
32:25
2 Peaks
0.
DC NL 0:00 RO
31:11
DC SN 31:25 RO
DC SN 31:48 RO
DC SN 31:57 RO
DC SN 32:29
1 Peak

0
DC NL 0:00 RO
DC SN 31:26 RO
32:04
1 Peak
0
DC NL 0:00
DC SN 31:27
32:04
DC SN 32:18 RO
1 Peak
1.23
1.24
2.42
1.64
0.31

05-1.43
0.87
0.93
1.38
1.24
1.20
5.96

88-1.20
4.06
1.09
0.61
1.09

37-0.51
1.63
0.42
0.58
0.70
1.06
0.39


. 88-1.20
2.74
0.81
1.04

.88-1.20
0.98
0.92
0.99
2.67

1,211.68 667.37
1,223.86 677.65
3.11
3.54
0.87
3,420.73

3.34
3.87
13.85
2,365.17 1,307.45
3,379.31 1.842.39
1.28
5,744.48
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1,324.95 692.08
3.12
894.39 466.29
2,219.34

0.91
1,874.76 555.58
5.08
2.36
1 .44
5.55
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0.86
6.18
872.46 444.26
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1.014
1.018
1.023

0.966-1.034
0.000
0.955
0.978
1,057.72 1.000 13C12-HXCDD 678
1,536.92 1.010 13C12-HXCDD 789
1.017

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0.000
632.87 1.001 1234678-HpCDF
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0.936-1.128
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1.025
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IS7


 'riangle Laboratories, Inc.® Analytical Services Division
 101 Capitola Drive • Durham, North Carolina 27713
 'hone: (919) 544-5729 • Fax: (919) 544-5491
                                                                   Printed: 12:03 09/18/97.
                                                                                   274

-------
Page No.      5
09/18/97

Compound/
M_2....  QC.Log  Omit Why
OCDF
442-444
        Listing of S975832B.dbf
        Hatched GC Peaks / Ratio /  Ret. Time
         .RT. OK Ratio Total.Area...  Area.Peak.1.. Area.Peak.2..  Rel.RT Compound,
                                                            0.884-1.116
                                                                0.000
                                                                0.919
                                                                0
                                                                                                      ic..
 442-444
0.76-1.02
DC
DC
DC
DC
DC
DC
DC
DC
DC
DC
DC
DC
DC

DC

NL
SN
SN
SN
SN
SN
SN
SN
SN
SN
SN
SN
SN

SN
1
0:
31:
32:
32:
32:
32:
32:
32:
33:
33:
33:
33:
34:
34:
35:
00
49
01
06
22
32
44
57
08
31
35
49
21
43
25
RO
RO

RO

RO .
RO

RO
RO
RO
RO


RO
0.
0.
0.
1.
0.
1.
1
0.
0
0
0
0
0
0
1
15
36
77
,62
,97
.14
.10
.86
.24
.39
.24
.30
.78
.88
.62
Peak
0
0
1
0
0
1
0
2
0
0
0
0
1
1.117
1
1,117
.17
.91
.01
.70
.61
.72
.76
.18
.45
.47
.68
.30
.57
.27
.49
.27
                                                           523.96
                                                                         593.31
                                                                  924
                                                                0.927
                                                                0.935
                                                                0.939
                                                                0.945
                                                                0.951
                                                                0.957
                                                                0.968
                                                                0.970
                                                                0.976
                                                                0.992
                                                                1.002 OCDF
                                                                1.023
                                                                                                      AN
 OCDD
 458-460
 458-460
               0.76-1.02
DC  NL   0:00 RO  6.29          0.13
DC  SN  34:21 RO  0.75          1.83
        34:38     0.83       1.049.26
      1 Peak                1.049.26
                                                           475.04
            0.884-1.116
                0.000
                0. 992
        574.22  1.000 OCDD
                                                                                                       AN
 13C12-OCDD                     0.76-1.02
 470-472         DC  NL   0:00 RO  9.71          0.13
                        34:38     0.87      2,111.51
 470-472               1 Peak                2.111.51
                                           983.01
                                                             0.995-1.005
                                                                 0. 000
                                                       1,128.50  1.000  13C12-OCDD
                                                                                       IS8
 Column Description.
                "Why" Code Description	  QC Log Desc.
 M_Z   -Nominal  Ion Mass(es)
 ..RT.  -Retention Time  (mmtss)
 Rat.l  -Ratio of M/M+2  Ions
 OK    -RO=Ratio Outside Limits
 Rel.RT-Relative Retention Time
     End of Report
                WL-Below Retention Time Window
                WH-Above Retention Time Window
                SN-Below Signal to Noise  Level
                
-------
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                                                        A6.76E6
                                                                              A6.37X6
                                                                                                   .2.5X6

                                                                                                   .1.9X6

                                                                                                   .1.3X6

                                                                                                   '.6.3X5
                                                                                                      0.0X0
   27:12 27:24 27:36 27:48  28:00  28:12 28:24 28:36  28:48  29:00 29:12 29:24 29:36  29:48 30:00 30:12
 rile:S975832 tl-406 Acq:ll-SEP-1997 11:39:38 XI+ Voltage SIX  70S lK>iae:583
  83.8639 T:3 BSOB(256,30, -3. 0) PKD(7,5,3, 0. OS\,2332.0,1. 00\,T, T) EiptEPCUS
 TRIANGLE LABS  Text:TLI LCSD   TLH43085                    IlKT. TIKE -   11:42
                                                                                                         Time
 1003

  80:

  60:

  40:

  30.

   0:
                                         A9.83E6
                                                         A9.73E6
                                                                              A8.31E6
                                                                                                   _ 3. 7E6

                                                                                                   .2.9E6

                                                                                                   .2.2E6

                                                                                                   .1.5E6

                                                                                                   .7.4E5
                                                                                                     O.OEO
                                                                                                        Tim
   27:12 27:24 27:36  27:48 38:00 28:12 28:34  38:36 28:48 39:00 29:12 29:24  29:36 29:48 30:00 30:12
 Fj.leiS975832 H-406 Acq:ll-SEP-1997 11:39:38  EI+  Voltage SIX 70S  SOiae:1059
 385.8610 T:3 BSOB(256,30,-3.0) PKS(7,5,3,0.05\,4236.0,1.00\,r,T)  Exp:EPCVS
 TSIAJfSLE LASS  Text.'IIJ LCSD   TLI#43085                     IXJ.  TIME -   11:42
 100$                                    A1.98E7          A1.95E7                                    -7.1E6
  80:

  60:

  40:

  so:

   0.
                                                                               Al.64E7
                                                                                                    .5.7E6

                                                                                                    .4.3E6

                                                                                                    .2.9E6

                                                                                                    .1.4E6
   27:12  27:24  27:36 27:48 28:00 28:12  28:24 28:36 28:48 29:00 29:12  29:24 29:36 29:48 30:00  30:12
 T±le:S975832 tl-406 Ac
-------
    27148    28:00   28tl2   28:24    28i36   28:48   29tOO    29tl2   29': 24   29': 36   29:48
 lle:S975832 tl-406 Acq:ll-SEP-1997 11:39:38 XI* Voltage SIX  70S Koi*»t296
 91.8127 r:3 BSUB(256,30,-3.0) PKD(7,5,3,0.05\,1184.0,L.OO\,r,T) Exp:EPCOS
TRIANGLE LABS  TextiTLI LCSD   TLIf 43085                    JKJ. TIMS -   Hi42
     27:48   28:00   28:12    28:24   28:36   28:48    29:00   29:12   29:24    29:36
rile:S975B32  tl-406 Acq:ll-SEP-1997 11:39:38 Eli- Voltage SIX  70S Noiae:927
 01.8558  F:3  BSUB(256,30, -3 . 0) PKD(7,5,3, 0. 05\,370S. 0,1.00%,T, T) ExpiEPCUS
TRIANGLE  LABS  Text:TLI LCSD   TLI#4308S                    rWJ. TIME -   lit42
lOOi                                                                     A1.84E7
   mian/iaj^ r±-4vo AcqilJ.-aff-J.yy' iiu>»j« fif  vt^Lfmgm SIM 7va HoitfUjy
 89.8156 T:3 BSUB(256,30,-3.0) PXD(7,5,3,0.OS\,1756.0,1.00\,T,T) ExpiXPCOS
  IAJKLE LABS  TfXtiTll LCSD   TLH430S5                     JKJ. TIM* -   11,42
 00*                                                         A6.67E6    A6.78E6
 ao:

 so:

 40.

 20.
                                                                                                ,.2.
                                                                              J1.4M

                                                                              '.9.6X5

                                                                              .4. US
 OOJ

 ao.

 60.

 40.

 20.
  0_
                                           A5.44E6
                                                                          A5.46E6
                              2.0X9

                              .1. 6X6

                              .1.2ft


                              .8.0E5

                              .4.0E5
                                                                      29:48
  so:

  so:

  
-------
ril«:SS 75832 tl-430 Acq: ll-SEP-1997 11:39:38 XI+ Voltage SIR 70S Hoi**: 15 8 5
407.7818 Ti4 3SV3(256,30,-3.0) PXD(7,5,3,0.05\,6340.0,1.00\,r,T) XxptEPCUS
TRIANGLE LABS TexttTLI LCSD TLI443085 1X7. TIME " 11:42
1004 A6.J2E6
80:
SO.
40.
20:
A
/ I A4.66X6
1 \ f^
\ A
l\ A
' 3lil2' ' ' 31»24 ' ' '31:36' '.31:48' ' ' 32:00 ' 32»12 32*24
rileiS975832 tl-430 Acq:ll-SEP-1997 11:39:38 XI+ Voltage SIR 70S Noia»:390
409.7789 P:4 3303(356, 30, -3 .0) PXD(7, 5,3,0. 05\,1S60 .0,1.00\,r,T) XxpiEPCUS
TRIANGLE LABS TttxtlTLI LCSD TLH43085 IKT. TIME • 11:42
1004 A6.33E6
80:
60:
40J
20:
0
rile
417.
TRIA
1003
80:
60:
40:
20:
0
rile
419.
TRIA
1003
sol
60.
40.
20.
0
rile
430.
TRIl
1001
80.
60.
40.
20.
0
rilt
479
TRIl
100.
SO.
60.
40.
20.
0
A
/ \ A4.28E6
II A
\ A
l\ i\
31\12 31:24 31:36 31:48 32:00 32:12 32:24
1S975832 tl-430 Acq:ll-SEP-1997 11:39:38 EH- Voltage SIR 70S Noiae:516
8253 r:4 BSUB(256,30, -3 .0) PKD(7, 5,3,0. 05\,2064 .0,1. 00\,r,T) Exp:EPCOS
NGLE LABS Tejct:TLI LCSD TLH43085 INJ. TIME - 11:42
AS . 56E6
A


/ V
31:12 31:24 31:36 31:48 32:00 32:12 32:24
•.S975832 tl-430 Acq: ll-SEP-1997 11:39:38 EH- Voltage SIR 70S Noiae:315
8220 F:4 BSUB ( 256 , 30, -3 . 0 ) PKD( 7, 5,3, 0 . 05\,1260. 0,1 . 00%, JT, T) Erp:EPCUS
NGLE LABS Taxt:2IX LCSD TLIt430S5 JK7. TIME * 11:42
Al . 32E7
A
A

\
/ V
31:12 31:24 31:36 31:48 32:00 32:12 32:24
'•.S975832 tl-430 Acq:ll-SEP-1997 11:39:38 EI+ Voltage SIR 70S
9729 r:4 ExptEPCUS
\NSLE LABS Text:TLI LCSD TLIt43085 JK7. TIKE - 11:42
•\f^-J^S*^-~^^^ — ^V^^^^^^-^^^y^



31:12 ' 31^24 ' ' 31:36' ' 31:48 ' ' 32:00 ' ' ' 32'tia' ' '32:24
i:S975832 tl-430 Acq: ll-SEP-1997 11:39:38 EH- Voltage SIR 70S
7165 F:4 ExpsEPCVS
WSLE LABS Text:TLI LCSD TLIt43085 IKT. TIME - 11:42
jj 31:43
: 31:31 |I
^x^WjJl^
31; 12 31i24 31:36 31t48 32:00 32:12 32': 24
-2.0I6
:



1.6X6
1.2X6
8.1X5
.4.1X5
.0.0X0
32i 36 32:48 Time
-1.9X6




32:36 32:48




321-36 32:48




' 32:36 ' ' ' 32:48 '
* 32; -.39
s/'-'-'S^- V^/^^"^



.1.5X6
.1.1X6
.7.6X5
.3.8X5
0.0X0
Time
.1.6X6
.1.3X6
'-.9.5X5
.6.4X5
.3.2X5
O.OEO
Time
3 . 8E6
.3.0X6
'.2.3X6
.1.5X6
.7.5X5
O.OEO
Time
2.8X6
.2.2E6
Ll . 7X6
.1 . 1X6
.S.5ES
O.OEO
32:36' ' ' 32:48 Time

32:42
32s 33 AAA l\J\n A
.1.1X4
.8.1X3
.5.4X3
.2.7X3
- O.OfO
32:36 32:48 Mae
282

-------
 'i±»,S975B33 91-430 Aoqill-sSf-1997  11,39,38  K*  Volt*?* SIS 703 «ol*e:577	
 23.7766 Tt4 BSUB(256,30,-3.0) PXD(7,5,3,0.OS\,2308.0,1.00\,T,T) XxpiXPCUS
TRIANGLE LASS  TextsTLI LCSD   TLIH3085                     XX7. TIMS -   11,42
 00%                                                      A4.44E6
 80.

 60.

 40.

 201
    31:18  31i24   31i30  31t36  31,42  31,48  31:54  32', 00  32:06  32,12   32,18
 ile:S975832  #1-430 Acq,ll-SEP-1997 11,39,38 XI* Voltage SIX 70S Soime,211
 25.7737 F:4  BSUB(256,30,-3.0) PKD(7,5,3,0.05%,844.0,1.00\,F,T) Xxp:EPCVS
TRIANGLE LABS  TextsTLI LCSD   TLH43085                    INJ. TIME -   1J j 42
 00\                                                      A4.28X6
  80.

  60.

  40.

  201
             ,4.1**

             .•.7X3

             .8.5X3

             14.3X3

             .2.1
                                                                                                '.9.
32,24  32,30
             -1.1X6

              '.». 4X5

              .6.3X3

              .4.2X5

              '.2.1E5
     31,18   31(24  31:30  31,36  31:42  31,48  31:54  32:00   32:06  32:12  32,18
 Tile:S975S32 »1-430 Aoqill-SEP-1997 11,39,38 EI+ Voltage SIS  70S HOiae,634
  35.8169 r-.4 BSUS(256,30,-3.0) PKD(7,5,3, 0. 05\,2536. 0,1. 00\,T, T) EzpsEPCOS
 TRIANGLE LABS  T*Xt,TLI LCSD   TLI#43085                    INJ. TIME -  11,42
 10 0\                                                    A9.21E6
  80J

  eo:

  401

  20.
32:24  32:30
     31,18  31,24  31:30  31:36  31:42   31:48   31:54  32:00  32:06  32:12  32:18
  •ile,S975832 tl-430 Acqsll-SEP-1997 11:39:38 EI+ Voltage SIX 70S Soiae:650
 437.8140 T:4 BSOB(256,30, -3.0) PKD(7,5,3,0.05\,2600.0,1.00\,T,T) ExptEPCUS
 TRIANGLE LABS  TextsTLI LCSD   TLIt43085                     ISJ. TIME -   111 42
 1001                                                     A9.26E6

  801


  60.


  401

  20.
 32:24  32:30
              .O.OEO
                  Time
               2.1E6

               1. 7E6

               .1.2E6

               .8.3X5

               .4.2X5

               .O.OEO
                  Tim.
     31:18  31:24  31,30   31,36   31:42  31:48  31:54  32:00  32,06   32,12  32,18  32:24  32,30
 rile:S975832 tl-430 Acq:ll-SEP-1997 11,39:38 EH- Voltage SIX 70S
 430.9729 T:4 ExpiEPCUS
 TRIANGLE LABS   Iext:TLI LCSD   TLI»43085                    INJ. TIME -   11:42
              .2.2X6

              11.8X6

              -1.3X6

               8.8X5

               4.4X5
 100*31:18
   80.

   60.

   40.

   20.

    0.
                  31,29
                                  31:42
                                                     31:58
                                                                     32:12
                                                                                          32:29
     31:18   31:24   31:30  31:36  31:42  31:48  31,54  32:00   32:06  32:12  32:18  32,24  32,30
               0.0X0
                  Tim
               2.6X6

               2.1X6

               .1. 6X6

               .1.1X6

               .5.3X5
                0.0X0
                   Tim
                                                                                                         283

-------
Til*tS975832 fl-430 Acq: ll-SEP-1997 11:39:38 XI+ Voltage SIX 70S Holfe:39
441.7428 ri4 BSOBf 250,30,-3.0> PKDf 7, 5,3,0.05%, 150. 0,1.
TSIAHGLX LABS T*xt:TLI LCSD TLH43085
1001
901
801
701
601
50.
40.
30:
20j
10J
01










4
31*00 32*00 	 33*00
00\,f,T) XXptXfCUS
Her. TIHX - 11*42
A5.24X6
ft







\
J V^
.ff.jrs
.0.225
.5.5*5
.4.8X5
.4.1X5
.3.4X5
.2.8X5
.2.1X5
.1.4X5
.0.9X4
0.0X0
34*00 35:00 £!••
File:S975832 fl-430 Acq: ll-SEP-1997 11:39:38 EH- Voltage SIR 70S Noise, 265
443.7399 T:4 BSUB(256,30, -3. 0) PKD(7 ,5,3,0 ,05\,1060 .0,1. 00\,T,T) XxpiEPCDS
TRIANGLE LABS Texts 1X1 LCSD 1X1*43085
100J
901
801
701
601
501
401
301
201
101
01











31:00 32:00 33:00
IKJ. TIME - 11*42
A5.93E6
\







\
J V
_8.0X5
_7.2X5
_5.4E5
L5.SX5
L4.8E5
L4.0X5
L3.2E5
.2.4X5
.1 . 5X5
.8.0X4
0.0X0
34:00 ' 35*00 	 Time
r±le:S975832 #1-430 Acq: ll-SEP-1997 11:39:38 EI+ Voltage SIR 70S
430.9729 T:4 ExptEPCUS
TRIANGLE LABS Text.-ZXI LCSD 0X1*43085
1003
901
801
70.
601
501
401
301
20.
!\ A ^(°9A 31:42 32:12 33:09
1 1 Jii ft* n iu AAJ\< kh> A »J^*Ji' i
V^W^^^
' i I* u rv VW VT v






i-o|
of
31:00 32:00 33*00

IWJ. TIME - 11:42

//WtfAMJlkKjVJlli-30 35l°9 ":44
^^^MAVW^^Y^
! " y v vy^ v \M







2.8X5
.2.5X5
^2.2X6
Ll . 9X6
Ll . 7X5
Ll . 4X5
Li.ixff
L8.3X5
L5.5X5
Is.ass
'• a . ox a
34:00 . 35:00 Time
f±le:S975832 fl-430 Acq: ll-SEP-1997 11:39:38 EH- Voltage SIR 70S
513.6775 T:4 ExptEPCUS
TRIANGLE LABS Text* 2X1 LCSD TLIf 43085
1001
90.
80.

70.
60.
SO.
40.
30.
20.
10.
0.


31 : 51



1 32*32 33*03

1 I31?" i , ll P
i i r. | | i. MI i
(yuMijUllL^
31*00 32:00 33*00

XK.T. TIMX - 11*42
33:3S 34 2i


34:45




>2Sl 34,11 35,04
1 II ll 1 1 1 1 II 35*27
yiy^
-.7.7X3
:7.0X3
L5.2X3

.5.4X3
.4.0X3
.3.9X3
.3.1X3
IE.2.3X3

1.7.7X2
t n nrn
34 >00 35*00 ri»«
284

-------
      34:24         34i30         34:36        34:42         34,48         34:54
 •±l»iS975832 tl-430 Acq:ll-SEP-1997 11:39:38 EH- Voltage SIX 703 Noi*»:37
 59.7348 F:4 BSDB(256,30,-3.0)  PKD(7,5,3,0.OS\,148.0,1.00\,f,T) XxptXPCUS
TRIANGLE LABS  Text < IXJ LCSD    TLIt43085                    1X7. TIKE -   11:42
 OOi,                                 A5.74E6
 BO:

 SO.

 40.

 20.
   **8975oj2 tl-430 Aoq111-SIP-1997 11:39:38 EIr Voltage SIM 70S Nairn*1221
 57.7377 rt4 BSVB(256,30,-3.0) PKO(7,5,3,0.05\,884.0,1.00\,T,T)  XxpiXTCOS
  IANGLX LABS  TmxttTLI LCSD   TLH43085                     IJKT. TIME -   Hi42
 00\                                 A4.
 80.

 SO.

 40.

 20.
                                       75X6
      34:24         34:30         34:36         34:42         34:48         34:54
 •±le:S975832 #1-430 Acq:ll-SEP-1997 11:39:38 EH- Voltaye SIS 70S NoiBe:342
469.7779 T:4 BSUB(256,30, -3. 0) PKD(7,5,3, 0.05\,1368. 0,1. 00\,T,T) Elp:EPCUS
TRIANGLE LABS  Text:IXI LCSD   TLIt43085                    IKT. TIME -   11:42
10 Oi:                                 A9.83ES
  so:
  so:
  40:
  20:
       34:24        34:30         34:36         34:42         34:48         34:54
rile:S975832 tl-430 Acq:ll-SEP-1997 11:39:38 EI+ Voltage SIR 70S Noiee:37
471.7750  r:4 BSUB(256,30r-3.0) PKD(7,5,3,0.05\,148.0,1.00\rr,T)  Cxp:EPCUS
TRIANGLE  LABS  TartsTLI LCSD   TLH43085                     IKJ. TIME -   II -.42
100\                             A1.13E7_

  80.

  SO.

  40.

  20.
      34:24         34:30         34:36         34:42         34:48         34:54
rile:S975832 tl-430 Acqtll-SEP-1997 11:39:38 EI+ Voltage SIR 70S
430.9729 f:4 ExpiEPCUS
TRIANGLE LABS  TextlTLI  LCSD   TLIt43085                    JWJ.  TINT -   11:42
       3±i24    _    34j^0                    34:41
                                                                                                -3.0*3

                                                                                                .4.50

                                                                                                .3.4*5

                                                                                                .2.3X3

                                                                                                .1.1X3
                                                                                        35100
e.txe
   ttmmk
                                                                                         35:00
                                                                                                 1.1E6

                                                                                                '.9. 2E5

                                                                                                .6.9E5

                                                                                                '.4.6ES

                                                                                                .2.3E5
                                                                                         35:00
                                                                                                 .O.OEO
                                                                                                     Tim
                                                                                                 .1.3E6

                                                                                                 .1. OE6

                                                                                                 _7.8E5

                                                                                                 ',5.2X5

                                                                                                 "-2.6ES
                                                                                          35:00
                                                                                                  .O.OEO
                                                                                                      Tim
  80.
  60.

  40.

  20.

   0.
                                                                                     34:58
       34:24
                     34:30
                                                                                                 -2.4E6

                                                                                                 -1.9E6

                                                                                                 L1.4E6

                                                                                                 .9.5X5

                                                                                                 .4.7X5

                                                                                                  0.0X0
                                   34:36
                                                 34:42
                                                               34:48
                                                                             34:54
                                                                                          351 00
                                                                                                        285

-------
                       fl=33U971
I Channel   I  338,3782     tak l.op
| Height  3,25 uoLts  Span   288 ppi

 Systei file naae
 Oka   file nate
 Resolution
 Group nmber
 lonlzatlon node
 Switching
 Ref, lasses   282,3825,
 fl  293      J   "331
 3  384      K   332
C   386
0   316
E   318
F   328
6   322
H   328
I   331
              L   334
              H   348
              H   342
              0   352
              P   354
              Q   356
              R   358
      2
     El*
 VOlTflGE
416,3768
S   368
T   379
I)   376
V   418
Ref, lass   416.9768     Peak top
         ,72 volts  Span   288 ppi
                                                                    286

-------
TLI Project:      43085
Client Sample:   TLI LCS
Method 23 PCDD/PCDF Analysis (a)
             Analysis File:  S975831
Client Project:
Sample Matrix:
TLI ID:

Sample Size:
Dry Weight:
GC Column:
S413-004
XAD
TLI LCS

1.000
n/a
DB-5

Date Received:
Date Extracted:
Date Analyzed:
Dilution Factor:
Blank File:
Analyst:

II
09/04/97
09/11/97
n/a
S975815
BJG

Spike File:
ICal:
ConCal:
% Moisture;
% Lipid:
% Solids:

SPX23704
SF56117
S975814
n/a
n/a
n/a
Ahalytes
2,3,7,8-TCDD
1,2,3,7,8-PeCDD
1,2,3,4,7,8-HxCDD
1,2,3,6,7,8-HxCDD
1,2,3,7,8,9-HxCDD
1,2,3,4,6,7,8-HpCDD
1,2,3,4,6,7,8,9-OCDD
2,3,7,8-TCDF
1,2,3,7,8-PeCDF
2,3,4,7,8-PeCDF
1,2,3,4,7,8-HxCDF
1,2,3,6,7,8-HxCDF
2,3,4,6,7,8-HxCDF
1,2,3,7,8,9-HxCDF
1,2,3,4,6,7,8-HpCDF
1,2,3,4,7,8,9-HpCDF
1,2,3,4,6,7,8,9-OCDF
internal Standards
l3C12-2,3,7,8-TCDF
3C,2-2,3,7,8-TCDD
l3C,2-l,2,3,7,8-PeCDF
!3C,2-l,2,3,7,8-PeCDD
13Ci2-l,2,3,6,7,8-HxCDF
13C,:-l,2,3,6,7,8-HxCDD
13C,2-l,2,3,4,6,7,8-HpCDF
13C,2-l,2,3,4,6,7,8-HpCDD
13C,2-1,2,3,4,6,7,8,9-OCDD
Amt (ng)
0.36
1.8
1.8
1.8
1.8
1.7
3.4
0.36
2.0
1.8
1.7
1.7
1.6
1.5
2.1
1.5
2.7
AmL (ng)
2.6
2.5
2.6
2.8
2.9
2.9
2.3
2.6
4.5
,0t EMPC

















% Recovery '
64.9
62.6
65.3
69.4
72.8
73.1
58.4
64.5
56.7

















QC Limits
40%-130%
40%- 130%
40%-130%
40%- 130%
40%-130%
40%-130%
25%-130%
25%-130%
25%-130%
ftatie
0.83
1.49
1.24
1.24
1.27
1.05
0.84
0.78
1.55
1.53
1.29
1.29
1.30
1.29
1.07
1.10
0.89
Ratio
0.76
0.82
1.52
1.44
0.49
1.23
0.43
1.03
0.85
fit
21:14
25:52
29:07
29:12
29:29
32:04
34:37
20:24
24:43
25:29
28:22
28:28
28:59
29:42
31:11
32:24
34:42
m
20:23
21:13
24:42
25:50
28:27
29:11
31:11
32:04
34:36
Ffeg*

	













	
—
Flags




	



	
                                        Page 1 of 2
                           X237_PSR T2.00. LARS 6.10.O
 Triangle Laboratories, Inc.®
 801 Capitola Drive • Durham, North Carolina 27713
 Phone: (919) 544-5729 • Fax: (919) 544-5491
                        Printed: 12:02

-------
TLI Project:       43085
Client Sample:    TLI LCS
                    Method 23 PCDD/PCDF Analysis (a)
                                  Analysis File:   S975831
Alternate Standards CType A>  , Arat
                        QC Limits , ,„. ..  Ratio,
                                                                                       Flags
13C12-l,2,3,7,8,9-HxCDF
13C,2-2,3,4,6,7,8-HxCDF
2.9
3.0
                                              72.3
                                              76.2
40%-130%
40%-130%
0.49
0.50
29:41
28:58
 Recovery Stamfords
                                      Ratk>
                                                                               srr
                               Ftegs
13C12-1,2,3,4-TCDD
13Ci2-l,2,3,7,8,9-HxCDD
                                       0.80
                                       1.21
                                                                              20:59
                                                                              29:28
                       Data Reviewer
                                               » , .• •
                                                                  09/18/97
                                            Page 2 of 2
                                                                                 X237J-SR vZOO.LARS6.IOW
Triangle Laboratories, Inc.®
801 Capitola Drive • Durham, North Carolina 27713
Phone: (919) 544-5729 • Fax: (919) 544-5491
                                             Printed: 12:02

-------
                       Initial
                                 ....Data...
Data Review By:
                                             Calculated Noise Area:  n/a
The Total Area for each peak with an ion abundance ratio outside
ratio limits has been recalculated according to method requirements.
Page No.
09/18/97
Listing of  S975831B.dbf
Matched GC  Peaks / Ratio / Ret.  Time
Compound/
M_Z.... QC.Log Omit Why ..RT. OX .Ratio Total.Area...  Area.Peak. 1.. Area.Peak.2..  Rel.RT Compound.Name..  ID..  Flag*.
TCDF
304-306
 304-306
0.65-0.89
DC
DC
DC

DC
DC

DC
DC
DC

ML
SN
SN

SN
SN

SN
SN
WH
2
0:
16:
18:
19;
19:
19:
20
21
22
22
00
55
53
:15
:30
:55
:24
:55
:15
-.41
RO
RO


RO


RO
RO
RO
1.
1.
0.
0.
1.
0.
0.
6
0
0
14
10
68
,37
.09
.66
.78
.53
.24
.46
Peaks
0.
0.
2.
44.
4.
19.
436.
0.
1.
1.
480.
12
92
35
31
07
67
34
30
54
79
.65
                                                            20.57
                                                           190.91
                                                   0.820-1.101
                                                       0.000
                                                       0.330
                                                       0.926
                                                 23.74  0.944
                                                       0.957
                                                       0.977
                                                245.43  1.001  2378-TCDF
                                                       1.075
                                                       1.092
                                                       1.113
                                                                                                      AN
 13C12-TCDF
 316-318
 316-318

DC
DC
DC
DC


DC


NL
WL
SN
SN


WH
2

0:
18:
19:
19:
20:
20
21

00
.04
:31
:55
:23
:53
-.43
0.
RO
RO
RO


RO
RO
65-
20.
1.
1.
0.
0.
0.
1
0.89
00
19
02
.79
.76
.95
.55
Peaks

0.
3.
8.
23.
3,872
26
3
3,899

11
.63
.30
.27
.82
.36
.27
.18
                                                    0.951-1.049
                                                        0.000
                                                        0.886
                                                        0.957
                                                        0.977
                                 1,677.61      2,195.21  1.000 13C12-2378-TCDF ISO
                                    14.17         14.89  1.025
                                                        1.065
                                       Above: TCDF /  TCDD Follows
 TCDD
 320-322
  320-322
0.65-
DC
DC
DC
DC
DC
DC
DC
DC
DC

DC
DC
DC
DC
DC

NL
SN
SN
SN
SN
SN
SN
SN
SN

SN
SN
WH
WH
WH
1
0:
18:
18:
18:
19:
19:
19:
20;
21
21
21
22
22
22
22
00
08
17
52
17
32
:53
;51
:00
:14
:46
:19
:29
:34
:48

RO

RO

RO
RO
RO


RO

RO
RO
RO
0.
1.
0.
0.
0.
1.
0.
2.
0,
0
0
0
1
1
2
0.89
75
18
84
32
74
38
29
.71
.83
.83
.13
.69
.63
.16
.02
Peak

0.
0.
1.
0.
1.
0.
2.
0.
1.
321
0
1
0
0
0
321

14
78
34
41
08
46
,51
.50
.90
.68
.71
.42
.90
.80
.83
.68
                                                            145.74
0.853-1.059
0.000
0.855
0.862
0.889
0.909
0.921
0.937
0.983
0.990
175.94 1.001
1.026
1.052
1.060
1.064
1.075









2378-TCDD





                                                                                                       AN
 Triangle Laboratories, Inc.® Analytical Services Division
 801 Cap'rtola Drive • Durham, North Carolina 27713
 Phone: (919) 544-5729 • Fax: (919) 544-5491
                                                                       Printed: 12:02 09/1J

-------
 Page No.
 09/18/97
Listing  of S975831B.dbf
Matched  GC Peaks / Ratio / R«t. Tin
 Compound/

 M_Z	 QC.Log Omit Why ..RT. OK Ratio  Total.Area... Area.Peak.1.. Area.Peak.2..  Rel.RT Compound. Name. . ID.
                                                                                                       Flags.
13C12-TCDD
332-334




332-334
PeCDF
340-342








340-342
13C12 -PeCDF
352-354







352-354
PeCDD
356-358









356-358
13C12-PeCDD
368-370


DC
DC





DC
DC



DC
DC

DC


DC

DC

DC
DC
DC
DC


DC
DC
DC
DC
DC
DC
DC
DC
DC
DC

DC
DC

NL
SN



3

NL
SN



SN
3N

SN
4

NL

SN

SN
SN
SN
SN
2

NL
SN
SN
SN
SN
SN
SN
SN
SN
WH
1
NL
SN

0:00
19:54
20:59
21:13
21:35
Peaks

0:00
23:21
23:50
24:21
24:43
25:01
25:21
25:29
26:27
Peaks

0:00
23:46
24:20
24:42
25:00
25:29
25: 50
26:26
Peaks

0:00
23:55
24:14
24:30
24:44
24:52
25:03
25:29
25:52
26:04
26:49
Peak
0:00
24:43
0.
RO
RO


RO

1.
RO
RO

RO

RO


RO

1.
RO

RO

RO

RO


1.
RO
RO

RO
RO
RO
RO
RO
RO
RO

1.
RO

65-0.89
41.
1.
0.
0.
0.

32-
1.
0.
1.
1.
1.
1.
1 .
1.
1.

32-
1 .
1.
1.
1.
1.
1.
0.
1.

.32-
3.
0.
1.
2.
2.
1.
0.
13.
1.
1.
1.

,32-
0.
1.
00
09
80 4
82 3
98
7
1.78
00
36
69
29
55 1
81
61
53 1
08
3
1.78
00
63
07
52 3
17
73
38
64
3
1.78
71
12
34
44
27
30
91
40
49 1
19
84
1
1.78
67
60
0.
15.
,527.
,018.
48.
,595.
Tf*nf
1 \~Ul
0.
i.
57,
31,
,871.
18,
1,
,701,
5,
,662.

0
33
12
,350
13
29
2
8
11
.06
,59 2,013.14
86 1,360.65
73 27.07
,18

,12
,18
.61 36.16
.72 19.28
.54 1,137.04
.92
.28
.84 1,028.85
.92
.71

.13
.25 20.62
.27
•64 2,023.45
.93
.76
.12
.98
0.906-1.094
0.
0.
2,514.45 0.
1,658.21 1.
27.53 1.

0.907-
0.
0.
21.45 0.
14.99 0.
734.50 1.
1.
1.
672.99 1.
1.

0.338-
0.
12.63 0.
0.
1.327.19 1.
1.
1.
1.
1.
000
938
989 13C12-1234-TCDD
000 13C12-2378-TCDD
017

1.078
000
945
965
986
001 12378-PeCDF
013
026
032 23478-PeCDF
071

1.162
000
962
985
000 13C12-P6CDF 123
012
032 13C12-PeCDF 234
046
070


RSI
IS1







AN


AN






IS2

SUR2


,383.89
PeCDF / PeCDD Follows --
0
1
2
0
4
5
3
0
,148
2
1
,148
0
5
.18
.12
.50
.99
.46
.30
.98
.26
•66 687.54
.42
.91
.66
.10
.96
0.921-1.026
0.
0.
0.
0.
0.
0.
0.
0.
461.12 1.
1.
1 .

000
926
938
948
957
963
970
986
001 12378-PeCDD
009
038









AN


0.845-1.155
0.000
0.
957

Triangle Laboratories, Inc.® Analytical Services Division
801 Caprtola Drive • Durham, North Carolina 27713
Phone: (919) 544-5729 • Fax: (919) 544-5491
                                                                  Printed: 12:02 0

-------
Page No.
09/18/97
Listing  of S975831B.dbf
Hatched  GC Peaks / Ratio / Ret. Time
Compound/
M_z.... QC.Log omit Why ..RT.  OK Ratio Total.Area... Area.Peak.1.. Area.Peak.2..  Rel.RT Compound.Name..  IB.. Tl*a*.
368-370
HxCDF
374-376









374-376
13C12-HXCDF
384-386









384-386
HxCDD
390-392









390-392
13C12-HXCDD
402-404





DC
DC
DC


DC

DC

DC


DC
DC


DC

DC
DC

DC


DC
DC
DC
DC
DC



DC
DC


DC
DC
DC

2

NL
SN
SN


SN

SN

WH
4

NL
SN


SN

SN
SN

SN
4

NL
SN
SN
SN
SN



WH
WH
3

NL
SN
SN

25:50
25:59
Peaks

0:
27:
27:
28:
28:
28:
28:
29:
29:
30:

00
23
30
22
28
40
59
09
42
03
1.

RO





RO

RO
1.
1.
44
46
1,995.
191.
2,186.
n«/*r^
19
37
56
1 / UuC
.05-1.43
1.
1.
1.
1.
1.
1.
1.
0.
1.
1.
35
51
25
29
29
13
30
91
29
58
Peaks

0:
27:
27:
28:
28:
28:
29:
29:
29:
29:

00
21
30
27
45
58
26
33
41
53
0.
RO



RO

RO
RO

RO
43-
0.
0.
0.
0.
1.
0.
0.
0.
0.
0.
Peaks

0:
28:
28:
28:
28:
29:
29:
29:
29:
29:

00
21
36
40
47
07
12
29
39
49
1.
RO
RO


RO



RO
RO
,05-
1.
2.
1.
1.
2.
1.
1.
1.
12.
2.
0.59
90
50
58
49
65
50
21
41
49
23

1.43
00
22
33
07
00
24
24
27
48
02
Peaks


1
0:00
28:
12
28:35
29:
ill

RO
3.
11.
25.
1,377.
1,761.
3.
1,326.
2.
1,126.
1.
5,591.

2.
15.
36.
2,657.
1.
2,573.
2.
2.
2,122.
2.
7,389.

1.
1.
5,
1,
1
918
1,111
1,074
0
2
3,104
17
13
51
64
25
82
00
26
66
93
55

64
07
40
14
65
38
46
61
29
64
21
p / tivf
' / nXf,
.97
.77
.97
.14
.30
.94
.83
.04
.65
.15
.81
.05-1.43
1.15
1.
1.
32
.01
1.23
3
2
15
2,203
.80
.09
.39
.22
1,178.84 816.35 1.000 13C12-PeCDD 123
113.72 77.65 1.006
•nV »— 1 T ftt^fr
0.955-1.052
0.000
0.963
0.967
775.40 602.24 0.997 123478-HxCDF
990.49 770.76 1.001 123678-HxCDF
1.008
748.24 577.76 1.019 234678-HxCDF
1.025
634-74 491.92 1.044 123789-HxCDF
1.056

0.359-1.141
0.000
0.961
13.29 23.11 0.967
873.82 1.783.32 1.000 13C12-HXCDF 678
1.011
853.16 1.720.22 1.018 13C12-HXCDF 234
1.035
1.039
702.08 .1,420.21 1.043 13C12-HXCDF 789
1.050

0.950-1.015
0.000
0.971
0.980
0.982
0.986
508.80 410.14 0.998 123478-HxCDD
615.10 496.73 1.001 123678-HxCDD
599.89 474.15 1.010 123789-HxCDD
1.016
1.022

0.966-1.034
0.000
0.966
0.979
1,214.42 988.80 1.000 13C12-HXCDD 678
IS3




AN
AN

AN

AN






IS4

ALT2


ALT1








AN
AN
AN







IS5
Triangle Laboratories, Inc.® Analytical Services Division
801 Capitola Drive • Durham, North Carolina 27713
Phone: (919) 544-5729 • Fax: (919) 544-5491
                                                                    Printed: 12:02

-------
page No.
09/18/97
Listing  of S975831B.db«
Matched  GC Peaks / Ratio / Ret. Time
Compound/
M_2.... QC.Log omit why ..RT. OK Ratio Total.Area... Area.Peak. 1.. Area.Peak.2.. Rel.RT Conpound.Name.. ID..  Flags.
402-404
HpCDF
408-410




408-410
13C12-HpCDF
418-420

418-420
HpCDD
424-426



424-426
13C 12 -HpCDD
436-438


436-438

OCDF
442-444









442-444
OCDD
458-460

458-460
2
DC NL

DC SN

DC WH
2
29:28
Peaks
1.21 3,029.99 1,661.33
5,233.21
XW.MM.. tt**tfTin / tiw*/*n9 9*0 1 Aue 	
0.88-1.20
0:00 RO 1.86
31:11
31:31 RO
32:24
32:45 RO
Peaks
1.07
0.55
1.10
0.74

nAWk/*s / n^sivksc' s wi A w«w 	
3.00
1,250.71 645.54
5.12
717.99 376.42
1.59
1,968.70
0.37-0.51
DC NL

1

DC NL
DC SN

DC WH
1

DC NL
DC SN

1


DC NL
DC SN
DC SN
DC SN
DC SN
DC SN
DC SN

DC SN
DC SN
0:00 RO
31:11
Peak
0.
0:00 RO
31:26 RO
32:04
32:16 RO
Peak
0.
0:00
31:26 RO
32:04
Peak

0.
0:00 RO
31:11 RO
31:44 RO
32:50 RO
33:34 RO
33:49 RO
34:13 RO
34:42
3 5 : 07 RO
35:28 RO
1.11
0.43

88-1.20
1.24
0.84
1.05
0. 65

88-1.20
1.08
1.39
1.03


.76-1.02
9.30
1.42
0.56
0.21
0.51
1.09
1.39
0.89
1.16
2.46
1 Peak

DC NL

0
0:00 RO
34:37
.76-1.02
6.00
0.84
1 Peak
1.37
1,570.80 471.35
1,570.80
HrsC^ni? / Ur%PnT"^ tTrtl 1 i*M*r« — —
tip*— Ur i ripv- ULj f o j. i ows — •*
1.77
7.75
724.96 370.95
1.73
724.96

3.27
12.12
1,592.57 809.60
1,592.57


0.09
1.47
0.62
0.59
1.40
1.74
1.42
914.71 431.72
1 .85
0.53
914.71

0.13
848.38 386.63
848.38
1,368.66 1.010 13C12-HXCDD 789
0.995-1.044
0.000
605.17 1.000 1234678-HpCDF
1.011
341.57 1.039 1234789-HpCDF
1.050

0.936-1.128
0.000
1,099.45 1.000 13C12-HpCDF 678

0.976-1.006
0.000
0.980
354.01 1.000 1234678-HpCDD
1.006

0.969-1.031
0.000
0.980
782.97 1.000 13C12-HpCDD 678


0.884-1.116
0.000
0.901
0.917
0.949
0.970
0.977
0.989
482.99 1.003 OCDF
1.015
1.025

0.884-1.116
0.000
461.75 1.000 OCDD

RS2

AN

AN




IS6




AN





IS7










AN





AN

 Triangle Laboratories, Inc.®  Analytical Services Division
 801 Cap'rtola Drive • Durham, North Carolina 27713
 Phone: (919) 544-5729 • Fax: (919) 544-5491
                                                                    Printed: 12:
97

-------
Page No.      5           Listing of S975831B.db«
09/18/97                 Hatched GC Peaks / Ratio / Ret.  Time

Compound/
M_Z.... QC.Log  Omit  Why ..RT. OK Ratio Total.Area... Area.Peak.1.. Area.Peak.2..  Rel.RT Compound. Name..  ID.. Flagc.

13C12-OCDD                    0.76-1.02                                     0.995-1.005
470-472         DC  ML   0:00 RO  2.17          0.79                             0.000
                DC  WL  34:22 RO  1.06          3.36                             0.993
                        34:36     0.85      1,782.44        820.90        961.54  1.000 13C12-OCDD      IS8
470-472               1 Peak               1,782.44
Column Description	   "Why"  Code Description	   QC Log Desc.
M_2   -Nominal Ion Mass(es)      WL-Below Retention Time Window   A-Peak Added
 ..RT. -Retention Time (mn:ss)    WH-Above Retention Time Window   K-Peak Kept
Rat.l -Ratio of M/M+2 Ions      SN-Below Signal  to Noise Level   D-Peak Deleted
OK    -RO=Ratio Outside Limits  
-------
ril»,S975831 #1-848 Acq:ll-SEP-1997 10:59>48 SI+ Voltagm SIR 70S Nairn* 1 38
303.9016 r>2 BSDB(256,30,-3.0) PKB(9,5,5,0.05\, 152.0, 1.00\,T,T) ExptXPCUS
TRIANGLE LABS TtxttTLI LCS TLH43085
1003
80:
60:
40:
20:
o:






17:00




A2.06E5
/\^
18:00 19:00
nur. TIMS -
A1.91E6




1 \
20:00 21:00
11:03






22:00
Tile:S975831 tl-848 Aoj:ll-SEP-1997 10:59:48 EH- Voltage SIR 70S Noitei34

-4 . 7S5





.3.8X5
-2. 8SS
.1.915
.9.5S4

Time

305.8987 T:2 BSUB(256,30,-3.0) PKD(9,5,5,0.05\r136.0r1.00\,r,T) ExptEPCUS
TRIANGLE LABS Text:TLI LCS TLH4308S
1003
80:
60:
40:
20:
o:






17:00




A2.37E5
/^
18:00 19:00
XWJ. TIMS -
A2.45E6




^ 1 ^
20:00 2l':00
11:03






22:00
rile :S9 75831 #1-848 Acqill-SEP-1997 10:59:48 EI+ Voltage SIR 70S Nbiae:601

-5.6S5





.4.4E5
'.3.3E5
-2.2E5
.LIES

Time

315.9419 T:2 BSUB(256, 30, -3. 0) PKD(9,5,5, 0. 05\,2404. 0,1 . 00\,T, T) Exp:EPCUS
TRIANGLE LABS TeJCt:TLI LCS TLI#43085 IJKT. TIME - 11-03
100^
80:
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40:
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331.9368 T:2 BSOB(256, 30, -3. 0) PXD( 7,5, 3, O.OS\,4916 . 0,1. 00%, T, 1) Exp:EPCUS
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333.9338 T:2 BSUB(256,30, -3 .0) PKD( 7,5, 3, 0. OS\,124 .0,1. 00\,F,T) Exp:EPCOS
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327.8847 F:2 BSVB(256, 30, -3 .0) PXJ>< 7,5,3, 0. 05\,156. 0,1. 00%,J-, T) EzpiEPCUS
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330.9792 T:2 Exp:EPCUS
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339.8597 Ti2 BSUB(256,30,-3.0) PKD(7,5,3, 0 .05\, 140 .0, 1.00\,T,T) XzptXPCUS
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341.8567 rt2 BSUB(256,30,-3.0) PXD(7,5,3,0.05\,136.0,1.00\,r,T) XipiXPCUS
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351.9000 Ts2 BSUB(256,30,-3 .0) PKD(7,5,3, 0. OS\,1S2. 0,1 . 00\,T,T) ExpsEPCUS
TRIANGLE LABS TejftsTLI LCS TLI#430S5
1003
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File:S975831 #1-848 Acqtll-SEP-1997 10:59:48
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353.8970 F:2 BSUB(256,30, -3 .0) PKD(7 ,5,3,0 .05\,156 .0,1. 00\,T,T) ExptEPCUS
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TiletS975831 #1-848 Acqsll-SEP-1997 10:59:48
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file,SS75BJl #1-040 Acqtll-SEP-1997 10l59l48 KI+ Voltage SIX 70S HOimmil32
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357.8516 F:2 BSUB(256, 30, -3. 0) PXD(7, 5,3,0. 05\,136 .0,1. 00\,F,T) XxptXPCUS
TRIANGLE LABS TextiXCT LCS TLH43085 INJ. TIMX - 11:03
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367.8949 F,2 BSUB(256, 30, -3.0) PKD(7, 5,3,0. 05\, 128. 0,1. 00\,F,T) ExpiEPCUS
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FiJ.eiS975B31 U-4O6 ACIJ, il-SXP-1997 1OI39HB £1+ Voltage SM  70S NOlfe,545
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TRIANGLE  LABS  Text:TLI LCS   TLI»43085                      IKJ. TIME -   11:03
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 TRIANGLE LABS  Text:TLI LCS    TLI#43085                     JK7. TIME -   11:03
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 TRIANGLE LABS  Text:TLI LCS   TLH43085                      IXJ. TIME -   11:03
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407.7818 F:4 BSOB(256, 30, -3. 0) PKD(7 ,5,3,0 .05\,5468. 0,1 .00\,r,T) XxptXPCOS
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409.7789 F:4 BSUB(256, 30, -3. 0) PKD(7,5, 3,0. 05\, 2944 .0,1 . 00\,F, I) Exp:EPCUS
TRIANGLE LABS Text-.TLI LCS TLIt43085 JJK7. TIME - 11:03
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417.8253 r-.4 BSVB(256,30,-3 .0) PKD(7 ,5,3,0 .OS\,2104 .0,1. 00\,T,T) Exp:EPCUS
TRIANGLE LABS Text:TLI LCS TLIt43085 IKT. TIME - 11:03
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File:S975831 tl-430 Acq:ll-SEP-1997 10:59:48 EI+ Voltage SIR 70S Noiae:475
419.8220 F:4 BSOB( 256, 30, -3 . 0) PKD( 7,5,3, 0.05\,1900. 0,1 . 00\,F, T) Exp:EPCUS
TRIANGLE LABS Text:TLI LCS TLIt43085 IKT. TIME - 11:03
1001
80.
60.
40.
20.
0.
A1.10E7
A
A

\
/ \
y v
31:12 31\24 31\36 31\4B 32\00 32\12 32\24^
File:S97S831 tl-430 Acq:ll-SEP-1997 10:59:48 EI+ Voltage SIR 70S
430.9729 F:4 Exp:EPCUS
TRIANGLE LABS Teit:TLI LCS TLIt43085 IKT. TIME - 11 .- 03
lOOi

80.
60.
40.
20.
0.
5-^\£M£f 31:14 ^i21 31,30 31i44 31:51 32:04 32,12 ,- ,0 33.
^ — ^-Ay — '^VN^.X^^ — N^\/>^A-/\/> — -~^~\fj\^r*^s*~^ 32L I/t~-^-<; /N





31:12 31:24 3l':36 31\48 32:00 32:12 32\24
rile:S97S831 tl-430 Acq: ll-SEP-1997 10:59:48 EH- Voltage SIR 70S
479.7165 F:4 Sip:EPCVS
TRIANGLE LABS Text:TLI LCS TLIt43085 IKT. TIKE - 11 : 03
100.
80.
60.
40.
20.
0.
\ 31,15 3a\°°
''•' \ 1
: | 31:39 |
: 31i33 I , „ , 32'24
• , h /i . L HA J L Al , » i
;A M^k /Vuw uU V\ 31A\ n\L /V\AA Wvl^i
:/W V/v VN 1 \J * W " v WV V \ 	 f\ \J« U ^V V V vW • v Y\XN
31:12 31:24 31:36 3l':48 32:00 32\12 32\24



-2. 0X6






.1.6X6
.1.2X6

.8.0X5
.4.0X5
0.0X0
32:36 32\48 Time



1 . 8X6






.1.5X6
.1.1X6

.7.3X5
.3 . 6X5
O.OEO
32\36 32l: 4 8 Time



1 . 6E6





ll.2E6
'•-9.3ES
:.6.2E5
.3.1E5
O.OXO
32\36 32*: 48 Time



3.5E6





.2.8E6
-2.1E6
.1.4E6
.6.9E5
'• o . OEO
32\36 32\48 Time



30 -2.6E6
~X .. 32:38
"Vvv — -^^—v^—





-2.1E6
.1 . 6X6
.1.1E6
.5 . 3X5
' 0 . OfO
32\36 ' ' ' 32\48 ' Time



cl . OS4

32:37
A A A A K
^K AMA AA
^/ LA/ v vw V\
.8.0X3
.6.0X3
.4 . 0X3
.2.0X3
• a - am
32s 36 32 1 48 Timi*

-------
Filt:S975831 tl-430 Acqtll-SXP-1997  10t59l4B EI+ Volt*y* SIX 70S HO1M»:542
423.7766 T>4 BSUB(256,30, -3. 0) PKD(7,5,3,0.05\,2168.0,1.00\,r,T) Xxp:XPCUS
TRIANGLE LABS  TuxttTLI JXS   TLH43085                     UU. TIM* -   11103
1003

 80.

 60.

 40.

 20:
                                                         A3. 71X6
    31:18  31t24   31:30  31:36  31:42  31:48  31:54   32:00  32:06  32:12  32:18
F±le:S97S831  tl-430 Acq:ll-SXP-1997 10:59i48 XI* Volt*g» SIX  70S Noita:435
425.7737 T:4  BSUB(256,30,-3.0) PKD(7,5,3,0.05\,1740.0,1.00\,r,T) ExptEPCUS
TRIANGLE LABS  TextjlXI LCS   TLH43085                     HKT. TIME -   11:03
1003k                                                       A3.54X6
  eo:

  60.

  40.

  20.
                                           -*.fM3

                                            f.9XS

                                           .3.1*5

                                           .3.4*5

                                           J..7X5
                                                                                                  0.0X0
                             32t24   32:30
                                           -8.4X5

                                           .6.7X3

                                           .5. 0X5

                                           '.3.4X5

                                           '.1. 7X5
                                                                                                  .O.OEO
     31:18   31:24  31:30  31:36  31:42   31:48  31:54  32:00  32:06  32:12   32:18
 rile:S975B31 tl-430 Acqsll-SSP-1997 10s59:48 EH-  Voltage SIX 70S Noiae:8S2
 435.8169 Ts4 BSUB(2S6, 30, -3. 0) PKJ>(7,5,3, 0.05%,3408. 0,1. 00\,T,T) Exp-.EPCUS
 TRIANGLE LABS  Text.-TtJ LCS   TLI#4308S                     JK7. TIME -   11 .• 03
 1004                                                     A8.J.OE6
  eo:
  40.
  20:
                              32:24  32:30
                                                Time
                                           -1.9E6

                                            .1. 5E6

                                            '.1. 1E6

                                            .7.5E5

                                            .3. 8E5
     31:18  31:24  31:30   31:36   31:42  31:48  31:54  32:00   32s06  32:12  32:18
 rile:S975831 tl-430 Acq:ll-SEP-1997 10:59:48 EI+ Voltage SIX  70S Koiee:786
 437.8140 T:4 BSUB(256,30,-3.0)  PKD(7,5,3, 0. 05%, 3144. 0,1. 00\,T, T) Ezp:EPCUS
 TRIANGLE LABS  TextsTLI LCS   TLI443085                     INJ". TIME -   11:03
 1004                                                     A7.83E6

  801

  60.

  40:

  20:
                              32:24   32:30
                                            .O.OEO
                                                Time
                                             1. 8X6

                                            .1.5X6

                                            '.1. 1X6

                                            '.7.3X5

                                            .3. 6X5
     31:18   31:24  31:30  31:36  31:42  31:48   31:54  32:00  32:06  32tl2   32:18  32:24  32,30
 File:S975831  tl-430 Acq:ll-SEP-1997 10:59,48  XI+ Voltage SIX 70S
 430.9729 F:4  ExptEPCUS
 TRIANGLE LABS  TextiZLX LCS   TLIt43085                      INJ. TIME -   11:03
                                             .O.OEO
                                                Time
  1003

   ao:

   60.

   40.

   20.

    01
31:58
      32:04
                32:12
                                 32:3532:30
r2.6E6

 .2.1E6

 .1.6E6


 .1. 0X6

 .5.2X5

 '.0.0X0
      31:18  31:24  31:30  31:36   31:42  31:48  31:54   32:00   32:06  32:12  32:18  32:24   32:30

-------
 ileiSS75831 #1-430 Adjtll-SXP-1997 10,59,48 EH- Voltage  SIX 70S Hoi*»:243
 41.7428 F,4 SSOB(256,30,-3.0)  PKD(7,5,3,0.05\,972.0,1.00\,T,T) XzptXPCVS
 SIANGLX LABS  TmjcttTLI LCS    TLH43085                      IKT. TIMX -   11:03
 OOi                                                                       A4.32X6
 901
 80.
 70-
 601
 501
 40.
 301
 301
         31:00             32x00              33:00              34:00             35 00
file.-S375831  #1-430 Acq:ll-3EP-1997 10:59,48 EI+ Voltage SIX 70S Noi*»i27
 43.7399 F:4  BSUB(356,30, -3. 0) PKD(7,5,3, 0. 05\,108. 0,1.00\,T, T) ExptEPCVS
TRIANGLE LASS  Text.-TEX LCS   TLII43085                      1X7. TIMX  -    11:03
                                                                                                      -5.1X5
                                                                                                      .4.5X5
                                                                                                      .4.0X5
                                                                                                      .3.5X5
                                                                                                      .3.0X5
                                                                                                      .2.5X5
                                                                                                      .3.0X5
                                                                                                      .l.SKS
                                                                                                      -1.0E5
                                                                                                      Li. 1X4
                                                                                                       .0. 0X0
                                                                                                          Tim,
1001
 901
 801
 701
 601
 501
 30.
 3Q.
                                                                           A4.83X6
                                                                                                       -S.9E5
                                                                                                       L5.JF5
                                                                                                       ''-4.7E5
                                                                                                       .4.1X5
                                                                                                       .3.5X5
                                                                                                       .3.9X5
                                                                                                       .2.3E5
                                                                                                       .1. 8X5
                                                                                                       .1.3X5
                                                                                                       .5.9X4
         31:00             32:00              33:00             34:00
File,S97SB31  #1-430 Acqtll-SEP-1997 10,59,48 EI+ Voltage SIS  70S
430.9729 F:4  EipiEPCUS
TRIANGLE LASS  Text:IIJ LCS   TLH4308S                      ItKT. TIME  -
J001^JJ^ /UA?" J. .  3i'44 33:0*
 901
 801
 70.
 60.
 501
 40.
 301
 20.
 lOjj
   0.
                                                                                  35:00
                                                                                                       '•.0.0X0
                                                                                                           Tim*
                                                                             111 03
                                                                                                35:47
          31:00             32,00             33\00             ' 34\00             '351-00
file:S575fl31 #1-430 Acq:ll-SEP-1997 10:59:48 EI+ Voltage SIR 70S
513.6775 F:4 ExpiEPCDS
TRIANGLE LABS  Text:TJtI LCS    TLIf43085                      TK7. TIME -   11:03
1001
                                                                                                       ^2.7X6
                                                                                                       .2.4X6
                                                                                                       .2.1X6
                                                                                                       _1.9X6
                                                                                                       :1.6X6
                                                                                                       ',1. 3X6
                                                                                                       .1. 1X6
                                                                                                       18.0X5
                                                                                                       .5.3X5
                                                                                                       .3.7X5
                                                                                                       .0.0X0
                                                                                                           Tim
                                                                                                       -1.2X4

-------
 'U»i£975B31 U-430 AaqtU-aXf-1997 10>59,48 XU- Volt*ym SIS 70S
 57.7377 r,4 BSUB( 256,30,-3.0)  PKD(7,5,3,0.05\,840.0,1.00\,T,T) XxpiEPCCB
TRIANGLE LASS  TmxtlTLI LCS   TLIt43085                     I1KT. TIM* -   11103
      34,24         34,30         34,36         34,42         34,48         34,54
 ile:S975831  41-430 Aoqill-SEP-1997 10,59,48 XI+ Voltage SIX  70S Noises37
 59.7348 F,4  BSUB(256,30,-3.0) PKD(7,5,3,0.05\,148.0,1.00\,T,T)  Exp:EPCDS
TRIANGLE LASS  TexttTLI LCS   TLH43085                     IHJ.  TIME -   11:03
 001                                 A4.62E6
       34,24         34,30         34:36         34:42         34:48         34:54
 ile:S975831  tl-430 Acq:ll-SEP-1997 10,59:48  EI+  Voltage SIX 70S Noise:451
 69.7779 T:4  BSUB(256,30, -3. 0) PKD(7,5,3, 0. 05\,1816. 0,1. 00\,T, T) ExpiEPCUS
 TRIANGLE LABS  TextsIXJ LCS   TLI#4308S                      inf. TIME -   11:03
  001                              A8.21E6
 00\
 so:
                                        7X6
       34:24         34:30         34,36         34:42         34:48         34:54
 r±la:S975831 U-430 Ac
-------
o
CO

-------
                      J , •=, ( <
                      --Li ci
CALIBRATION
       DATA
             Triangle Laboratories, Inc.
       801 Capitola Drive      P.O. Box 13485
       Durham, NC 27713-4411     Research Triangle Park, NC 27709-346
       919-544-5729         Fax #919-544-5491
                               305

-------
Date: 09/12/97
  TRIANGLE LABORATORIES, INC.
Continuing Calibration for S975861
Operator 	
• MT,
Init Calibration. : SF56117
ICal Date 	
Analyte Summary
Name

Total MCDF

Total MCDD

Total DCDP

Total DCDD

Total TriCDF

Total TriCDD

2378-TCDF

TOTAL TCDF
2378-TCDD

TOTAL TCDD
12378-PeCDF

23478-PeCDF
TOTAL PeCDF
12378-PeCDD

TOTAL PeCDD
123478-HxCDF

123678-HxCDF
234678-HxCDF
123789-HxCDF
TOTAL HxCDF
123478 -HxCDD
• 06/10/97
RF Ratio

0

0

0

0

0

0

1

1
1

1
1

1
1
1

1
1

1
1
0
1
0
162
.000

.000

.000

.000

.000

.000

.182 0.81

.182 0.81
.078 0.79

.078 0.79
.051 1.53

.100 1.52
.075 1.52
.210 1.59

.210 1.59
.070 1.33

.354 1.31
.059 1.32
.981 1.34
.116 1.33
.908 1.25
Instrument
Std.Conc . - -

RT RT Rel. RT

: S


ICal
RF
i *J '



50.00


Delta
RF

%D


Lo/High
1:
15
2:
16
8:
16
9:
17
12
19
14
20
18
23

19
23

23
27


24
27

28
30




34
:34
19
:19
34
:34
19
:19
:34
:34
:19
:19
:05 21:35 1.0008
:33

:31 22:20 1.0007
:32

:27 25:38 1.0007
:30
26:22 1.0293

:45 26:43 1.0000
:22

:02 29:09 0.9971
:42
29:15 1.0006
29:45 1.0177
30:27 1.0416

28:32 29:52 0.9972
2

1

0

1

1

0

1

1
1

1
1

1
1
1

1
1

1
1
1
1
0
.087

.625

.687

.326

.082

.933

.251

.251
.191

.191
.111

.115
.113
.256

.256
.215

.574
.247
.105
.285
.953
-2

-1

-0

-1

-1

-0

-0

-0
-0

-0
-0

-0
-0
-0

-0
-0

-0
-0
-0
-0
-0
.087

.625

.687

.326

.082

.933

.069

.069
.113

.113
.060

.015
.038
.046

.046
.145

.220
.188
.124
.169
.045
100

100

100

100

100

100

-5

-5
-9

-9
-5

-1
-3
-3

-3
-11

-14
-15
-11
-13
-4
.0%

.0%

. 0«

.0%

.0%

.0%

.5%

.5%
.5%

.5%
.4%

.4%
.4%
.7%

.7%
.9%

.0%
.1%
.2%
.1%
.7%
30:23
123678-HxCDD
1
.059 1.25

29:57 1.0000
1
.133
-0
.074
-6
.6%
Page 1
Triangle Laboratories, Inc.® Analytical Services Division
501 Capitola Drive • Durham, North Carolina 27713
'hone: (919) 544-5729 • Fax: (919) 544-5491
                                                            Printed: 22:27 09/12/97
                                                                       306

-------
Continuing Calibration for S975861
123789-HxCDD
TOTAL HxCDD
1234678 -HpCDF

1234789 -HpCDF
TOTAL HpCDF
1234678-HpCDD

TOTAL HpCDD
OCDF

OCDD

1.090
1.019
1.503

1.267
1.385
0.934

0.934
1.597

1.040

1.25
1.25
1.03

1.03
1.03
1.00

1.00
0.86

0.85


30:14 1.0095
1.091 -0.001
1.059 -0.040
31:44
33:15


31:59
32:54

31:16
39:16
31:16
39:16
31:54 1.0000

33:05 1.0371

32:44 1.0000


35:25 1.0043

35:17 1.0005

Other Standard Summary
Name

37C1-TCDD

13C12-PeCDF 234

13C12-HxCDF 478
13C12-HxCDF 234
13C12-HXCDF 789
13C12- HxCDD 478
13C12- HpCDF 789

Internal Standard
Name

13C12-2378-TCDF

13C12-2378-TCDD

13C12-PeCDF 123

13C12-PeCDD 123

13C12-HXCDF 678

13C12- HxCDD 678


RF

0.842

0.975

0.934
0.903
0.789
0.950
0.830

Ratio
162


1.54

0.50
0.49
0.49
1.21
0.42

RT
Lo/High
20:19
24:19
21:37
29:37




29:54
35:54
RT Rel. RT

22:20 1.0007

26:21 1.0286

29:09 0.9971
29:44 1.0171
30:27 1.0416
29:52 0.9972
33:04 1.0366

Summary
RF

1.488

1.131

1.302

0.780

1.171

0.934


Ratio
1&2
0.76

0.80

1.53

1.52

0.50

1.21


RT
RT Rel. RT
1.543 •

1.184
1.363
1.068

1.068
1.493

1.105

ICal
RF

0.843

0.970

0.959
0.926
0.805
0.973
0.771

ICal
RF
•0.040

0.083
0.022
-0.134 -

-0.134 -
0.104

-0.065

Delta
RF

-0.001

0.005

-0.025
-0.023
-0.016
-0.023
0.059

Delta
RF
-0.1%
-3.8%
-2.6%

7.0%
1.6%
12.6%

12.6%
7.0%

-5.9%


%D

-0.1%

0.5%

-2.6%
-2.5%
-2.0%
-2.4%
7.6%


%D
Lo/High
20:34
22:34
20:19
24:19
21:37
29:37
22:43
30:43
25:14
33:14
28:57
30:57
Page
21:34 1.0000

22:19 1.0000

25:37 1.0000

26:43 1.0000

29:14 1.0000

29:57 1.0000

2
1.318

1.066

1.133

0.635

1.204

0.995


0.170

0.065

0.169

0.145

-0.033

-0.061


12.9%

6.1%

14.9%

22.9%

-2.7%

-6.1%


Triangle Laboratories, Inc.® Analytical Services Division
801 Capitola Drive • Durham, North Carolina 27713
Phone: (919) 544-5729 • Fax: (919) 544-5491
Printed:
222ft 09*tt/9:

-------
13C12-HpCDP 678   0.831  0.42

13C12-HpCDD 678   0.786  1.10

13C12-OCDD        0.453  0.94
Continuing Calibration for S975861
          29:54  31:54 1.0000   0.887 -0.056  -6.3%
          35:54
          31:44  32:44 1.0000   0.815 -0.029  -3.5%
          33:44
          35:07  35:16 1.0000   0.519 -0.066 -12.6%
          35:27
Recovery Standard Summary
Name               RF   Ratio
13C12-1234-TCDD   1.000  0.81

13C12-HXCDD 789   1.000  1.21
           RT
                         162    Lo/High
              ICal    Delta
 RT   Rel.  RT  RF       RF    %D

22:08 0.9918   1.000   0.000    0.0%

30:14 1.0095   1.000   0.000    0.0%
                      QC Front End Check:
                       1.4500
                                 Page
 Triangle Laboratories, Inc.®  Analytical Services Division
 301 Capitola Drive • Durham, North Carolina 27713
 3hone: (919) 544-5729 • Fax: (919) 544-5491
                                                               Printed: 2257

-------
                       Continuing  Calibration  for S975839
Operator 	 :
Init Calibration.:
ICal Date 	 :
Analyte Summary
Name

Total MCDF

Total MCDD

Total DCDF

Total DCDD

Total TriCDF

Total TriCDD

2378-TCDF

TOTAL TCDF
2378-TCDD

TOTAL TCDD
12378 -PeCDF

23478-PeCDF
TOTAL PeCDF
12378-PeCDD

TOTAL PeCDD
123478-HxCDF

123678-HxCDF
234678-HxCDF
123789-HxCDF
TOTAL HxCDF
123478 -HxCDD

123678 -HxCDD
i W ? / A. */ " •
KAS
: SF56117
• 06/10/97

RF Ratio
142
0.000

0.000

0.000

0.000

0.000

0.000

1.207 0.83

1.207 0.83
1.189 0.78

1.189 0.78
1.124 1.53

1.147 1.52
1.136 1.53
1.282 1.59

1.282 1.59
1.145 1.29

1.490 1.30
1.117 1.30
1.028 1.31
1.195 1.30
0.896 1.21

1.056 1.23




RT
Lo/High
0:21
14:21
1:10
15 : 10
7:21
15:21
8:10
16:10
11:21
18:21
13:10
19:10
16:39
22:24

18:01
22:24

22:20
26:35


23:44
26:27

27:10
29:54




27 : 42
29:35

Instrument. . :
Std.Conc . . . :
Related CCal:
ICal
RT Rel. RT RF

2.0

1.6

0.6

1.3

1.0

0.9

20:22 1.0008 1.2

i.:
21:12 1.0016 1.]

i.:
24:42 1.0007 l.j

25:27 1.0311 1.:
i.:
25:50 1.0006 1.:

i.:
28:21 0.9965 1.

28:27 1.0000 1.
28:58 1.0182 1.
29:41 1.0434 1.
1.
29:06 0.9977 0.

29:11 1.0006 1.
                                                               50.00
                                                              RF    %D


                                                       2.087  -2.087  100.0%


                                                       1.625  -1.625  100.0%


                                                       0.687  -0.687  100.0%


                                                       1.326  -1.326  100.0%


                                                       1.082  -1.082  100.0%


                                                       0.933  -0.933  100.0%


                                                       1.251  -0.044   -3.5%


                                                       1.251  -0.044   -3.5%


                                                       1.191  -0.002   -0.2%


                                                       1.191  -0.002   -0.2%


                                                       1.111   0.013    1.1%


                                                       1.115   0.032   2.9%


                                                       1.113   0.023   2.0%


                                                       1.256  0.026   2.1%


                                                       1.256  0.026   2.1%


                                                       1.215 -0.070  -5.8%


                                                       1.574 -0.084  -5.3%


                                                       1.247 -0.130 -10.4%


                                                       1.105 -0.077  -7.0%


                                                       1.285 -0.090  -7.0%


                                                       0.953 -0.057 -6.0%


                                                       1.133  -0.077  -6.8%
                                 Page
Triangle Laboratories, Inc.® Analytical Services Division
801 Capitola Drive • Durham, North Carolina 27713
Phone: (919) 544-5729 • Fax: (919) 544-5491
Printed: 19:23

-------
                       Continuing Calibration for S975839
123789 -HxCDD
TOTAL HxCDD
1234678-HpCDF
1234789-HpCDF
TOTAL HpCDF
1234678-HpCDD
TOTAL HpCDD
OCDF

OCDD

1.039
0.997
1.482
1.168
1.325
1.047
1.047
1.498

1.055

1.24
1.23
1.06
1.07
1.07
1.05
1.05
0.89

0.86

29:28 1.0103
31:00 31:11 1.0000
32:33
32:24 1.0390
31:16 32:03 1.0005
32:12

30:38 34:44 1.0029
38:38
30:38 34:37 0.9995
38:38
Other Standard Summary
Name

37C1-TCDD

13C12-PeCDF 234

13C12-HXCDF 478
13C12-HXCDF 234
13C12-HXCDF 789
13C12- HxCDD 478
13C12 -HpCDF 789

Internal Standard
Name

13C12-2378-TCDF

13C12-2378-TCDD

13C12-PeCDF 123

13C12-PeCDD 123

13C12-HXCDF 678

13C12-HXCDD 678


RF

0.968

0.963

0.946
0.875
0.770
0.905
0.778

Ratio
162


1.56

0.50
0.49
0.49
1.21
0.42

RT RT Rel. RT
Lo/High
19:10 21:12 1.0016
23:10
20:41 25:26 1.0304
28:41
28:20 0.9959
28:57 1.0176
29:40 1.0428
29:05 0.9971
29:11 32:23 1.0385
35:11
Summary
RF

1.526

1.045

1.054

0.556

1.419

1.032


Ratio
162
0.76

0.80

1.53

1.45

0.51

1.23


RT RT Rel. RT
Lo/High
19:21 20:21 1.0000
21:21
19:10 21:10 1.0000
23:10
20:41 24:41 1.0000
28:41
21:49 25:49 1.0000
29:49
24:27 28:27 1.0000
32:27
28:10 29:10 1.0000
30:10
Page 2
1.091 -0.052
1.059 -0.062
1.543 -0.061
1.184 -0.016
1.363 -0.038
1.068 -0.021
1.068 -0.021
1.493 0.005

1.105 -0.050

ICal Delta
RF RF

0.843 0.125

0.970 -0.007

0.959 -0.013
0.926 -0.051
0.805 -0.035
0.973 -0.068
0.771 0.007

ICal Delta
RF RF

1.318 0.208

1.066 -0.021

1.133 -0.079

0.635 -0.079

1.204 0.215

0.995 0.037


-4.8%
-5.9%
-4.0%
-1.3%
-2.8%
-1.9%
-1.9%
0.3%

-4.5%


%D

14.8%

-0.7%

-1.4%
-5.5%
-4.3%
-7.0%
0.9%


»D

15.8%

-1.9%

-7.0%

-12.5%

17.9%

3.7%


Triangle Laboratories, Inc.® Analytical Services Division
801 Capitola Drive • Durham, North Carolina 27713
Phone: (919) 544-5729 - Fax: (919) 544-5491
Printed: 19:
ISI

-------
13C12-HpCDF 678   0.880  0.43

13C12-HpCDD 678   0.713  1.00

13C12-OCDD        0.456  0.87
Continuing Calibration for S975839
          29:11  31:11 1.0000   0.887 -0.007  -0.8%
          35:11
          31:02  32:02 1.0000   0.815 -0.102 -12.6%
          33:02
          34:26  34:38 1.0000   0.519 -0.063 -12.2%
          34:46
Recovery Standard Summary
Name               RF   Ratio
                         162
13C12-1234-TCDD   1.000  0.81

13C12-HXCDD 789   1.000  1.23
           RT
         Lo/High
             ICal   Delta
RT   Rel. RT  RF      RF
%D
                 20:58 0.9906   1.000  0.000   0.0%

                 29:28 1.0103   1.000  0.000   0.0%
                      QC  Front  End  Check:
                       1.7362
                                 Page
Triangle Laboratories, inc.® Analytical Services Division
801 Capitola Drive • Durham, North Carolina 27713
Phone: (919) 544-5729 • Fax: (919) 544-5491
                                                               Printed:

-------
                       Continuing Calibration for S975814

Init Calibration.
ICal Date 	
Analyte Summary
Name

Total MCDF

Total MCDD

Total DCDF

Total DCDD

Total TriCDF

Total TriCDD

2378-TCDF

TOTAL TCDF
2378-TCDD

TOTAL TCDD
12378 -PeCDF

23478-PeCDF
TOTAL PeCDF
12378 -PeCDD

TOTAL PeCDD
123478-HxCDF

123678-HxCDF
234678 -HxCDF
123789-HxCDF
TOTAL HxCDF
123478-HxCDD

123678-HxCDD
• JM
: SF56117
• 06/10/97

RF Ratio
1&2
0.000

0.000

0.000

0.000

0.000

0.000

1.118 0.80

1.118 0.80
1.146 0.80

1.146 0.80
1.093 1.53

1.143 1.50
1.118 1.51
1.209 1.59

1.209 1.59
1.097 1.28

1.379 1.29
1.073 1.27
0.977 1.29
1.132 1.28
0.855 1.23

1.058 1.24
Tnst* Tiinwfcnt' . . • S



RT
Lo/High
0:24
14:24
1:13
15:13
7:24
15:24
8:13
16:13
11:24
18:24
13:13
19:13
16:44
22:28

18:06
22:28

22:24
26:38


23:47
26:30

27:11
29:56




27:44
29:37

Std.Conc
Related

RT Rel. RT













20:25 1.0008


21:14 1.0008


24:43 1.0007

25:29 1.0317

25:52 1.0013


28:22 0.9965

28:28 1.0000
28:59 1.0181
29:41 1.0427

29:07 0.9977

29:12 1.0006
. . . . : 50.00
CCal: S975778
ICal Delta
RF RF %D

2.087 -2.087 100.0%

1.625 -1.625 100.0%

0.687 -0.687 100.0%

1.326 -1.326 100.0%

1.082 -1.082 100.0%

0.933 -0.933 100.0%

1.251 -0.133 -10.6%

1.251 -0.133 -10.6%
1.191 -0.045 -3.8%

1.191 -0.045 -3.8%
1.111 -0.018 -1.6%

1.115 0.028 2.5%
1.113 0.005 0.5%
1.256 -0.047 -3.7%

1.256 -0.047 -3.7%
1.215 -0.118 -9.7%

1.574 -0.195 -12.4%
1.247 -0.174 -13.9%
1.105 -0.128 -11.6%
1.285 -0.153 -11.9%
0.953 -0.098 -10.3%

1.133 -0.075 -6.6%
                                 Page   1
Triangle Laboratories, Inc.® Analytical Services Division
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Phone: (919) 544-5729 • Fax: (919) 544-5491
Printed: 03:o3)l/f!/97

-------
Date: oa/ii/a/
123789 -HxCDD
TOTAL HxCDD
1234678-HpCDF
1234789-HpCDF
TOTAL HpCDF
1234678- HpCDD
TOTAL HpCDD
OCDF

OCDD






XK.LAnUArf£« A«fV7Wi\«**WJX.tAJl-»
Continuing Calibration
1.052 1.24 29:29
0.989 1.24
1.384 1.04 31:01 31:11
32:33
1.094 1.05 32:23
1.239 1.04
1.001 1.03 31:16 32:03
32:13
1.001
1.470

1.049

1.03
0.88

0.90


30:
38:
30:
38:

32
32
32
32

34:39

34:32

for S975814
1.0103 1.091
1.059
1.0000 1.543
1.0385 1.184
1.363
1.0005 1.068

1.

1.


0034

0000

Other Standard Summary
Name

37C1-TCDD

13C12-PeCDF

13C12-HXCDF
13C12-HXCDF
13C12-HxCDF
13C12- HxCDD
13C12- HpCDF





234

478
234
789
478
789

Internal Standard
Name



13C12-2378-TCDF


13C12-2378-TCDD

13C12-PeCDF

13C12-PeCDD

13C12-HxCDF

13C12-HXCDD


123

123

678

678

RF

0.972

1.014

0.955
0.886
0.798
0.897
0.787

Ratio
142


1.54

0.50
0.49
0.49
1.22
0.43

RT
RT
Rel. RT
1.068
1.493

1.105

ICal
RF
-0.039
-0.070
-0.159 -
-0.090
-0.124
-0.067
-0.067
-0.023

-0.056

Delta
RF
-3.5%
-6.7%
10.3%
-7.6%
-9.1%
-6.3%
-6.3%
-1.5%

-5.1%


%D
Lo/High
19:
23:
20:
28:




29:
35:
13
13
42
42




ill
:11
21:13

25:28

28 : 21
28:58
29 : 41
29:06
32:22

1.

1.

0.
1.
1.
0.
1,

0000

0310

9959
0176
0427
9971
.0379

Summary
RF

1.554

1.110

1.243

0.713

1.294

0.964

Ratio
1&2
0.74

0.78

1.52

1.58

0.50

1.22

RT
RT
Rel. RT
0.843

0.970

0.959
0.926
0.805
0.973
0.771

ICal
RF
0.129

0.044

-0.004
-0.040
-0.007
-0.076
0.016

Delta
RF
15.3%

4.5%

-0.4%
-4.3%
-0.8%
-7.8%
2.1%


%D
Lo/High
19
21
19
23
20
28
21
29
24
32
28
30
:24
:24
:13
:13
:42
:42
:50
:50
:28
:28
:11
:11
20:24

21:13

24:42

25:50

28:28

29 : 11

1

1

1

1

1

1

.0000

.0000

.0000

.0000

.0000

.0000

1.318

1.066

1.133

0.635

1.204

0.995

0.236

0.044

0.110

0.078

0.090

-0.031

17.9%

4.2%

9.7%

12.3%

7.5%

-3.1%

                                Page
Triangle Laboratories, Inc.® Analytical Services Division
801 Capitola Drive • Durham, North Carolina 27713
Phone: (919) 544-5729 • Fax: (919) 544-5491
Printed; 03:04 09/11/9
         313

-------
Date:

13C12-HpCDF 678   0.876  0.45

13C12-HpCDD 678   0.782  1.06

13C12-OCDD        0.434  0.84
Continuing Calibration for S975814
          29:11  31:11 1.0000    0.887  -0.011  -1.3%
          35:11
          31:02  32:02 1.0000    0.815  -0.033  -4.1%
          33:02
          34:22  34:32 1.0000    0.519  -0.085  -16.3%
          34:42
Recovery Standard Summary
Name               RF   Ratio
13C12-1234-TCDD   1.000  0.83

13C12-HXCDD 789   1.000  1.22
           RT
             ICal    Delta
RT   Rel.  RT  RF      RF
%D
                         1&2    Lo/High
                 21:00 0.9898   1.000   0.000    0.0%

                 29:29 1.0103   1.000   0.000    0.0%
                      QC Front End Check:
                       1.6171
                                 Page
Triangle Laboratories, Inc.® Analytical Services Division
801 Capitola Drive • Durham, North Carolina 27713
Phone: (919) 544-5729 • Fax: (919) 544-5491
                                                             Printed: 03:04 09/11/97
                                                                        314

-------
                       Continuing Calibration for P973843
Analysis Date	: 09/12/97
Operator	: WK
Init Calibration.: PF22206
ICal Date	: 02/20/96
Analysis Time	: 11:04
Analyte Summary
Name

2378-TCDF

TOTAL  TCDP

2378-TCDD

TOTAL  TCDD
                          Method	: C2NP
                          Instrument..: P
                          Std.Conc....:       5.00

                          GC Column...: DB-225

                                    ICal    Delta
 RF   Ratio
RT
RT   Rel.  RT  RF
                             RF
%D
       1&2    Lo/High
0.964  0.76    16:14  20:40  1.0008    1.040  -0.076   -7.3%
               22:38
0.964  0.76                          1.040  -0.076   -7.3%

1.001  0.75    17:03  19:28  1.0009    0.992   0.009    0.9%
               22:00
1.001  0.75                          0.992   0.009    0.9%
 Other Standard Summary                                ICal    Delta
 Hame               RF   Ratio     RT     RT    Rel.  RT   RF      RF    %D
                          1&2    Lo/High
 37C1-TCDD         0.937          17:27  19:28  1.0009    1.014 -0.077  -7.6%
                                  21:27

 Internal Standard Summary                             ICal   Delta
 Name               RF   Ratio     RT     RT    Rel.  RT  RF      RF    %D
                          1&2    Lo/High
 13C12-2378-TCDF   1.201  0.77    19:39  20:39  1.0000   1.388 -0.187 -13.5%
                                  21:39
 13C12-2378-TCDD   1.006  0.79    17:27  19:27  1.0000   1.067 -0.061  -5.7%
                                  21:27

 Recovery Standard Summary                              ICal   Delta
 Name               RF   Ratio     RT     RT   Rel. RT  RF      RF    %D
                          1&2    Lo/High
 13C12-1234-TCDD   1.000  0.82           19:41 1.0120   1.000   0.000    0.0%
                                  Page
 Triangle Laboratories, Inc.® Analytical Services Division
 801 Caphola Drive • Durham, North Caiotna 27713
 Phone: (919) 544-5729 • Fax: (919) 544-5491
                                                                    Printed: 11:46 09/1
                                                          : 11:4609/1^97

-------
                                          ur
                      Continuing  Calibration for P973859
lalysis  Date....:  09/13/97
aerator	:  JM
lit Calibration.:  PF22206
:al Date	:  02/20/96
aalysis  Time....:  10:24
                                           Method	: C2NF
                                           Instrument..: P
                                           Std.Conc	:        5.00

                                           GC Column...: DB-225
nalyte Sumnary                                       ICal   Delta
sine               RF   Ratio     RT     RT   Rel.  RT  RF      RF    %D
                        1&2    Lo/High
                 0.949  0.76    16:14  20:40 1.0008   1.040 -0.091  -8.7%
                                22:37
                 0.949  0.76                          1.040 -0.091  -8.7%
378-TCDF

3TAL TCDF

378-TCDD

3TAL TCDD
                 1.077  0.86    17:02  19:28 1.0017   0.992  0.085   8.5%
                                22:00
                 1.077  0.86                          0.992  0.085   8.5%
ther Standard Suntnary                                ICal   Delta
ame               RF   Ratio     RT     RT   Rel. RT  RF      RF    %D
                        1&2    Lo/High
7C1-TCDD         0.928          17:26  19:28 1.0017   1.014 -0.086  -8.5%
                                21:26

nternal Standard Sunsnaxy                             ICal   Delta
ame               RF   Ratio     RT     RT   Rel. RT  RF      RF    %D
                        1&2    Lo/High
3C12-2378-TCDF   1.265  0.77    19:39  20:39 1.0000   1.388 -0.123  -8.9%
                                21:39
3C12-2378-TCDD   0.984  0.79    17:26  19:26 1.0000   1.067 -0.083  -7.8%
                                21:26

ecovery Standard Sumnary                             ICal   Delta
ame               RF    Ratio      RT     RT   Rel. RT  RF       RF    %D
                         1&2    Lo/High
3C12-1234-TCDD   1.000   0.81           19:40 1.0120   1.000   0.000    0.0%
                                Page
 tangle Laboratories, Inc.®  Analytical Services Division
 )1 Caprtola Drive • Durham, North Carolina 27713
 Tone: (919) 544-5729 • Fax: (919) 544-5491
                                                                                    Printed: 11 -32 09/13/97
                                                                                                 316

-------
                    Initial calibration sunnary tot
Analysis Date	: 02/20/96
Instrument	: P
                         Method	
                         GC Column..
                          C2NF
                          DB-225
Analytes
2378-TCDF
TOTAL TCDF
2378-TODD
TOTAL TCDD

Otner Standards
37C1-TCDD
 RF     SD   %RSD
1.040 0.109   10%
1.040 0.109   10%
0.992 0.101   10%
0.992 0.101   10%
 RF     SD
1.014 0.048
%RSD
  5%
          RT
        21:32
       RT/LO
       14:31
RT/HI
25:31
        20:12  16:11   24:11
Ratiol
 0.767
 0.767
 0.782
 0.782
                                                                     Ratio2
 N
10
10
10
10
  RT   RT/LO  RT/HI  Ratiol  Ratio2   N
20:12  18:11  22:11                 10
 Internal Standards  RF     SD   %RSD      RT   RT/LO  RT/HI  Ratiol  Ratio2   N
 13C12-2378-TCDF    1.388 0.062    4%    21:31  20:31  22:31   0.758          10
 13C12-2378-TCDD    1.067 0.036    3%    20:11  18:11  22:11   0.786          10

 Recovery Standards  RF     SD   %RSD      RT   RT/LO  RT/HI  Ratiol  Ratio2   N
 13C12-1234-TCDD    1.000 0.000    0%    20:27                 0.794          10
         of Report **
                                  Page
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801 Capftoia Drive • Durham, North Carolina 27713
Phone: (919) 544-5729 • Fax: (919) 544-5491
                                                                 Printed: 23:10

-------
 Instrument
 Analytes
 Total  MCDF
 Total  MCDD
 Total  DCDF
 Total  DCDD
 Total  TriCDF
 Total  TriCDD
 2378-TCDF
 TOTAL  TCDF
 2378-TCDD
 TOTAL  TCDD
 12378-PeCDF
 23478-PeCDF
 TOTAL  PeCDF
 12378-PeCDD
 TOTAL PeCDD
 123478-HxCDF
 123678-HxCDF
 234678-HxCDF
 123789-HxCDF
 TOTAL HxCDF
 123478-HxCDD
 123678-HxCDD
 123789-HxCDD
 TOTAL HxCDD
 1234678-HpC
 1234789-HpC
 TOTAL HpCDF
 1234678-HpC
 TOTAL HpCDD
 OCDF
 OCDD
  37C1-TCDD
t ,
1
1
1
IDF
IDD
i
)
)F
3F
)F
3D
3D
:DF
:DF
:DF
:DF
3F
:DD
:DD
:DD
3D
?CDF
?CDF
DF
pCDD
DD


ndards

DF 234
DF 478
DF 234
DF 789
:DD 478
:DF 789
Standards
8-TCDF
'8-TCDD
IDF 123
S
RF SO %RSD
2.087 0.000 0%
1.625 0.000 0%
0.687 0.000 0%
1.326 0.000 0%
1.082 0.000 0%
0.933 0.000 0%
1.251 0.116 9%
1.251 0.116 9%
1.191 0.231 19%
1.191
1.111
1.115
1.113
1.256
1.256
1.215
1.574
1.247
1.105
1.285
0.953
1.133
1.091
1.059
1.543
1.184
1.363
1.068
1.068
1.493
1.105
RF
0.843
0.970
0.959
0.926
0.805
0.973
0.771
RF
1.318
1.066
1.133
0.
0.
0.
0.
0.
0.
0.
0.
0.
0.
0 .
0.
0.
0.
0.
0.
0.
0,
0
0
0
0

0
0
0
0
0
0
0

0
0
0
231
082
061
069
113
113
064
099
069
060
062
067
070
067
067
,103
,100
.095
.089
.089
.131
.066
SD
.038
.030
.042
.021
.044
.027
.049
SD
.065
.020
.051
19%
7%
5%
6%
9%
9%
5%
6%
6%
5%
5%
7%
6%
6%
6%
7%
8%
7%
8%
8%
9%
6%
%RSD
5%
3%
4%
2%
5%
3%
6%
%RSD
5%
2%
5%
vw
RT
8:15
8:42
10:38
11:09
13:59
14:03
19:43
20:36

24:
24:

25:

27:
28:
28:
29:

28:
28:
29:


12
59

22

55
01
32
15

41
46
03

30:45
RT/LO
0:01
0:34
6:43
7:34
10:43
12:34
15:43
16:34

20:11


21:21

24:01




24:45



26:45
RT/HI Ratiol Ratio2
13:43 2.931
14:34 2.827
14:43 5.965
15:34 1.609
17:43 1.025
18:34 1.064
23:43 0.799
0.799
24:34 0.772

28:


29:

32:




32:



34:

11


21

01




45



45
31:57

31:


:37

34:09
34
:03
RT
20
24
27
28
29
28
31

19
20
24
:36
:58
:55
:32
:15
:40
:57
RT
:43
:34
:11

27:36

30:02
30:02
RT/LO
18:34
22:11




28:45
RT/LO
18:43
18:34
20:11

35:

38
38

:36

:02
:02
RT/HI
22
26




34
:34
:11




:45
RT/HI
20
22
28
:43
:34
:11
0.772
1.552
1.470
1.509
1.526
1.526
1.247
1.260
1.243
1.246
1.249
1.265
1.251
1.233
1.249
1.034
1.080
1.053
0.993
0.993
0.376
0.902
Ratiol Ratio2

1.470
0.518
0.517
0.519
1.241
0.424
Ratiol Ratio2
0.734
0.802
1.447
N
1
1
1
1
1
1
5
5
5
5
5
5
5
5
5
5
5
5
5
5
5
5
5
5
5
5
5
5
5
5
5
N
5
5
5
5
5
5
5
N
5
5
5
                                  Page
Triangle Laboratories, Inc.® Analytical Services Division
801 Capitola Drive • Durham, North Carolina 27713
Phone: (919) 544-5729 • Fax: (919) 544-5491
Printed: 09:49 06/10/9".
         318

-------
13C12-PeCDD 123    0.635 0.082   13%    25:21  21:21  29:21   1.461            5
13C12-HXCDF 678    1.204 0.073    6%    28:01  24:01  32:01   0.522            5
13012-HxCDD 678    0.995 0.017    2%    28:45  27:45  29:45   1.240            5
13C12-HpCDF 678    0.887 0.046    5%    30:45  28:45  34:45   0.429            5
13C12-HpCDD 678    0.815 0.077    9%    31:36  30:36  32:36   1.019            5
13C12-OCDD         0.519 0.080   15%    34:02  32:02  36:02   0.866            5

Recovery Standards  RF     SD   %RSD      RT   RT/LO  RT/HI   Ratiol   Ratio2   M
13C12-1234-TCDD    1.000 0.000    0%    20:21                 0.811            5
13C12-HXCDD 789    1.000 0.000    0%    29:02                 1.231            5

•»* End of Report •**
                                  Page
Triangle Laboratories, Inc.® Analytical Services Division
801 Caprtoia Drive • Durham, North Carolina 27713                                         Printed: 09:49 06/1C
Phone: (919) 544-5729 • Fax: (919) 544-5491                                                       o 1 Q

-------
      Appendix C.3




     Analytical Data




Method 29 Multiple Metals

-------

-------
                           CASE NARRATIVE
       Analysis of Samples for the Presence of Trace Metals
                          Method 29 April 1996 Rev.
             Client:
Pacific Environmental Services
             TLI Project Number:      43411


             Date:                     November 1,1997
                        This report should only be reproduced in full.
                  Any partial reproduction of this report requires permission from
                              Triangle Laboratories, Inc.
Rev. 07-May-97
                                             Triangle Laboratories, Inc.
                                 801 Capitola Drive            P.O. Box 13485
                                 Durham, NC 27713-4411        Research Triangle Park, NC 27709-3485
                                 919-544-5729                Fax # 919-544-5491

-------
Triangle Laboratories, Inc.                                         November*!, Iff?
Case Narrative                                                TLI Project #: 43411

Overview

Six train samples and a blank train sample were analyzed for silver (Ag), arsenic (As),
barium (Ba), beryllium (Be), cadmium (Cd), cobalt (Co), chromium (Cr), copper (Cu),
manganese (Mn), nickel (Ni), phosphorus (P), lead (Pb), antimony (Sb), selenium (Se),
thallium (Tl), zinc (Zn), and mercury (Hg). For all analyses, the samples and associated
QC samples were prepared and analyzed following the guidelines of Method 29 April
1996 Rev. Results reported relate only to the items tested.

PC Remarks

The release of this set of data by Triangle Laboratories,  Inc. was authorized by the Quality
Control Chemist who has reviewed each sample data package individually following a
series of inspections/reviews. When applicable, general deviations from acceptable QC
requirements are identified below and comments are made on the effects of these
deviations upon the validity and reliability of the results. Specific QC issues associated
with this particular project are:

Sample Receipt:

Seven train samples were received without tocilant on September 26,1997 in good condition.
The sample I-M29-2-BHAR was received, but this sample was not listed on the client' schain-
of-custody.

Sample Preparation:

Laboratory documentation of the sample preparation is included in the data package.

Instrumentation:

 Silver (Ag), arsenic (As), barium (Ba), beryllium (Be), cadmium (Cd), cobalt (Co),
 chromium (Cr), copper (Cu),  manganese (Mn), nickel  (Ni), phosphorus (P), lead (Pb),
 antimony (Sb), selenium (Se), and zinc (Zn) concentrations were determined by
 Inductively Coupled Plasma Emission Spectroscopy (ICP).

 Thallium (Tl) concentrations were analyzed by Graphite Furnace Atomic Absorption
 (GFAA).

 Mercury (Hg) concentrations were determined by Cold Vapor Atomic Absorption
 (CVAA).

-------
Triangle Laboratories, Inc.                                          November 1,1997
Case Narrative                                                 TLI Project #: 43411

The linear range for the instrument TJA 61E Trace Analyzer was based on four standards
and a blank, which established a correlation coefficient value greater than or equal to
0.995.  A calibration curve, based on a blank and one standard, is established for each
analytical run, followed by a check high standard and an initial calibration verification
(ICV). The check high standard does not deviate from the calibration curve by more than
5%.  In addition, continuing calibration verifications (CCVs) are performed throughout
the analytical run.

A Reporting Detection Limit (RDL) is used instead of an Instrument Detection Limit
(DDL). The spectrometer and atomic absorption instruments can achieve low detection
limits between 0.2-8 ppb levels for many analytes.  Triangle Labs is using RDL values of
1-10 times the IDL as detection limits for reporting purposes.

Data Review:

All analytes found in the method blank (MB) are detected at a level equal to or less than
the respective Reporting Detection Limits (RDLs) except for Ni. The following guidelines
may be used to assess analyte concentrations relative to the method blank: 1. Analyte
quantitations should be considered valid if the level of blank contamination is less than five
percent of the level detected in the field sample, 2. Analyte quantitations should be
considered estimated if the analyte level in the sample is five to twenty times the level of
the analyte in the blank, or 3. Analytes whose level in a sample is the same as or less than
five times the level detected in the associated blank should be considered present likely
due to laboratory contamination and not native to the sample.  Please note that the Ni
results that are near the RDL should be considered biased high.

The laboratory control sample (LCS) for Ni and Tl demonstrated percent recoveries
outside the QC criteria of 80-120 percent. Please note that the sample results  should be
considered biased high for Ni and biased low for Tl. No sample was available for a second
preparation.

All samples were received outside of the 28 day sampling to analysis holding time for Hg,
therefore the holding time for Hg could not be met. All samples were analyzed within the
six month sampling to analysis holding time for all other requested analytes.

The sample IDs on the client chain-of-custody did not match with the IDs on the sample
containers. The sample IDs on TLI's chain-of-custody matches the IDs on the sample
containers. The sample IDs on the Hg spreadsheets for the KMnO4 and HCI containers do
not have the addition description added in order to alleviate redundancy.

-------
Triangle Laboratories, Inc.                                        November 1,1997
Case Narrative                                              TLI Project #: 43411

The concentrations for Tl demonstrated high negative numbers for the samples analyzed
by ICP, therefore the samples were analyzed by GFAA in order to obtain better results. A
duplicate analysis is not reported for elements analyzed by GFAA. The GFAA instrument
analyzes two separate aliquots of the sample and averages the values for a final result.
These two analyses agree within a RPD of 20% or a second ran is done for that sample.
The ICP instrument analyzes one continuous aliquot three times and averages the values
for a final result. The ICP does not take two separate aliquots, therefore a DA is
performed.

The serial dilution results for Cr for the sample O-M29-1-FHACE,FHAR,FILTER FH
demonstrated a RPD outside the QC control criteria of 10.0 percent, which indicates the
presence of an amount of interferents specific to this analyte in the native sample matrix.
Please note that the post-digestion spike (PDS) for Cr demonstrated a percent recovery
within QC criteria, which indicates no significant amount of interfences specific to this
analyte in the native sample matrix. Also note that this sample should be considered
biased low for Cr due to matrix interferences.

The post-digestion spike (PDS) for Co for the sample O-M29-1-FHACE,FHAR,FILTER
FH demonstrated a percent recovery outside the QC criteria, which  may indicate
significant matrix effects specific to this analyte in the native sample matrix. Please note
that this sample should be considered biased low for Co due to matrix interferences.

The recoveries for the post-digestion spike (PDS) are not reported for Ba and Mn for
sample O-M29-1-FHACE,FHAR,FILTER FH. The spike concentrations added were
insignificant in comparison to the levels of these analytes present in  the native sample.

The pre-digestion spike (MS) and the pre-digestion spike duplicate  (MSD) for Hg for the
samples O-M29-1-HNO3 BH, O-M29-2-HN03 BH, I-M29-1-HNO3 BH, I-M29-2-
HNO3 BH, and I-M29-3-HNO3 BH demonstrated percent recoveries outside the QC
criteria, which may indicate significant matrix effects specific to this analyte in the native
sample matrix. Please note that samples O-M29-1-HNO3 BH, O-M29-2-HNO3 BH and
I-M29-1-HNO3 BH should be considered biased low due to matrix interferences. Also
note that samples I-M29-2-HNO3 BH and I-M29-3-HNO3 BH should be considered
biased high due to matrix interferences.

QC requirements:

The duplicate analyses for analytes analyzed by ICP cannot be considered valid qualifiers if
the concentrations of the analytes in the original and/or duplicate sample are not at least
ten times the respective RDLs. The RPDs for these analyses are indicated by or "
-------
Triangle Laboratories, Inc.                                          November 1,1997
Case Narrative                                                 TLI Project*: 43411

For duplicate analyses which are valid qualifiers, the quality control RPD is ± 20.0
percent. If RPDs are outside this range, interferences are suspected.

The serial dilution analyses for analytes analyzed by GFAA cannot be considered valid
qualifiers if the concentrations of the analytes in the serial dilution sample are not at least
five times the respective RDLs. The serial dilution RPDs for these analyses are indicated
by "
-------
                     TRIANGLE LABORATORIES, INC.

                LIST OF CERTIFICATIONS AND ACCREDITATIONS
ENVIRONMENTAL

American  Association for Laboratory Accreditation. Accredidation pending.  Certificate
Number 0226-01. Accreditation for technical competence in Environmental Testing.(Including
Waste Water, Sol/Haz Waste, Pulp/Paper, and Air Matrices) Parameters are AOX/TOX, and
Dioxin/Furan. Method 1613 for Drinking Water.

State of Alabama,  Department of Environmental Management.   Expires December 31,
1997. Laboratory I.D. # 40950. Dioxin in drinking water.

State of Alaska, Department of Environmental Conservation. Expires December 21, 1997.
Certificate  number OS-00397. Dioxin in drinking water.

State of Arizona,  Department of Health Services.   Expires May 26, 1998. Certificate
#A20423. Drinking Water for Dioxin, Dioxin in WW and S/H Waste.

State of Arkansas, Department of Pollution Control and Ecology. Expires February 18,
1998. Pulp/paper, soil, water, and Hazardous Waste for Dioxin/Furan; AOX/TOX.

State of California, Department of Health Services.  Expires August 31,  1999. Certificate
#1922. Selected Metals in Waste Water; Volatiles, Semi-volatiles, and Dioxin/furan in  WW and
Sol/Haz Waste. Dioxin in drinking water.

State of Connecticut, Department of Health Services.  Recertification pending. Registration
#PH-0117. Dioxin in drinking water.

Delaware  Health and Social Services.  Expires December  31, 1997. Certificate #NC 140.
Dioxin in drinking water.

Florida Department of Health and Rehabilitative Services.  Expires June 30, 1998.Dioxin in
DW. Drinking Water ID HRS# 87424. Metals, Extractable Organics (GC/MS), Pesticides/PCB's
(GC) and Volatiles (GC/MS) in  Environmental Samples.   Environmental water  ID HRS#
E87411.

Hawaii Department of Health.  Expires March 1, 1998. Dioxin in drinking water. "Accepted"
status for regulatory purposes .
Revised 10/28/97 RM
Printed 10/29/97                                   Triangle Laboratories, Inc.
Pnnted 10/29/97
                                   Durham, NC 27713-4411        Research Triangle Park, NC 27709-348
                                   919-544-5729                Fax #919-544-5491

-------
Idaho Department of Health and Welfare.  Expires November 30, 1997. Dioxin in drinking
water.

State of Kansas, Department of Health and Environment.   Expires January 31,  1998.
Environmental Analyses/Non potable Water and Solid and Hazardous Waste.  Method 1613
for drinking water. ID #'s - Drinking water and/or pollution control - E-215. Solid or Hazardous
Waste-E-1209.

Commonwealth  of  Kentucky,  Department for  Environmental  Protection.    Expires
December 31, 1997. ID#90060. Dioxin in drinking water.

Maryland  Department of Health and  Mental Hygiene.  Expires September 30,  1998.
Certification #235. Drinking water by Method 1613A.

State of Michigan, Department of Public Health.  Expires June 3, 1998. Drinking water by
Method 1613.

Mississippi State Department of Health.  No expiration date..  Dioxin in drinking water.

Montana Department of Health and Environmental Services.  Expires December 31, 1997.
 Dioxin in drinking water.

State of New Jersey, Department of Environmental Protection and Energy.  Extended by
state. Temporary certificate until December 31, 1997. ID #67851. BNAs and Volatiles. Dioxin in
drinking water.

State of New Mexico,  Environment Department.  Recertification pending. Dioxin in drinking
water.

New York State Department of Health. Expires  April 1, 1998. ID  #11026. Environmental
Analyses of  non-potable Water, Solid and Hazardous Waste. Method 1613 in DW.

State of North Carolina, Department of  Environment Health and  Natural Resources
Expires August 31, 1999. Certificate # 37751. Dioxin in drinking water.

State of North Carolina, Department of Environment, Health,  and Natural Resources,
Division of Environmental Management.  Expires December 31, 1997. Certificate # 485.
Metals, pesticides & PCBs, semi-volatiles and volatiles; TCLP.

North Dakota  State  Department of Health and Consolidated Laboratories.   Expires
December 31, 1997.  Certificate # R-076. Effective October 4, 1993.  Dioxin in drinking water.
Revised 10/28/97 RM

Printed 10/29/97

-------
Oklahoma Department of Environmental Quality.  Expires August  31,  1998.  Laboratory
#9612. Dioxin by 1613A, 8290 and 8280.

State of South Carolina, Department of Health and Environmental Control.  Expires April 1,
1998. Certificate  number #99040001  (drinking water). Expires August 31, 1999. Certificate
number #99040002 (other parameters). Dioxin/Furans, BNA, Volatiles, and PCBs/pesticides
under Clean  Water Act, 2,3,7,8-TCDD for Drinking Water, and Organic extractables for Solid
and Hazardous Waste.

State of Tennessee.  Department of  Environment and Conservation. Expires February 5,
1999. ID #02992.  Method 1613 Drinking water only.

U.S. Department of Agriculture Soil Permit.  Expires September 30, 2001. Permit No.  S-
3790. Under the authority of the Federal Plant  Pest Act,  permission is granted to receive
foreign soil samples for use in laboratory analysis.

U.S. Army Corps of Engineers.  Expires November 30, 1997.  Validated to perform methods
8280 & 8290 for Lockboume Landfill  Site  Investigation, Defense Distribution Depot Projects,
and assorted projects  for the USAGE North Pacific Division Laboratory.

U.S. EPA Region V.  Expires November 14, 1999. Dioxin in drinking water.

U.S. EPA Region VIII, for the State of Wyoming.  Expires November 13, 1997.  Dioxin in
drinking water.

State of Utah, Department of Health. Expires December 31, 1997. Certificate Number E-166.
Certification for the following parameters:  Semi-Volatiles and Volatiles under RCRA; Volatiles
under Clean Water Act; Dioxin/furans by Method 8280; Drinking water for Dioxin by Method
1613; Metals including Mercury and Microwave Digestion.

Commonwealth  of Virginia, Department of General Services, Division of  Consolidated
Laboratory Services. Expires June 30, 1998. ID #  00341. Dioxin in drinking water.

State  of  Washington,  Department of Ecology.   Expires September  11,  1998.  Lab
Accreditation  Number  C067.  Scope  of  Accreditation  applies  to water  analyses   for
Polychlorinated Dibenzo-p-dioxins and Polychlorinated Dibenzofurans,  BNA Extr (Semivolatile)
Organics and Purgeable (Volatile) Organics.

State of Washington, Department of Health. Expires April 30, 1998. Dioxin in drinking water.
  Lab I.D. 129

State of West Virginia, Department  of Health.  Expires December 31, 1997.  Certificate No.
9923(C). Dioxin in drinking water.
 Revised 10/28/97 RM

 Printed 10/29/97
                                                                                     8

-------
State of Wisconsin,  Department  of  Natural  Resources.  Expires August  31,  1998.
Laboratory  ID  Number 999869530. Certification for the  following categories  of  Organics:
Purgeable, Base/Neutral, Acid, PCBs, and Dioxin. Expires  November 14, 1999. Laboratory ID
999869530. Dioxin in drinking water.

PHARMACEUTICAL

Drug Enforcement Agency (DEA).   Expires November  30, 1997.  Registration  number
RT01195835. Controlled substance registration for schedules 1,2,3,3N,4,5.

N.C. Department of Human Resources.  Expires October 31, 1998.  Registration  number
NC-PT 0000 0031. North Carolina controlled substances registration. Application submitted for
renewal.

Food &  Drug Administration (FDA)  Registration.   Expires June  1998.  ID  #'s  001500
1053481. Annual registration of drug establishment. Annual registration of drug establishment.

OTHER

Clinical Laboratory Improvement Amendments (CLIA) Registration.  Expires May 30, 1999.
ID # 34D0705123.   Department  of Health  & Human  Services,  Health  Care  Financing
Administration.

U.S. EPA Large Quantity Hazardous  Waste Generator.    No expiration  date.   EPA ID
#NCD982156879. Permit indicates that the laboratory is a large generator of hazardous waste.

North Carolina Radioactive Materials  License.  Expires April 30 1998. License No. 032-
0954-1. License authorizes the licensee to receive, acquire, own, possess, transfer, import and
use such radioactive materials as designated.

North Carolina General License for Radiation Protection.  No. expiration date. License No.
032-875-OG.   The  general license applies only to  radioactive material contained in  devices
which have been manufactured and labeled in accordance with specific requirements.
Revised 10/28/97 RM

Printed 10/29/97
                                                                                 9

-------
                               ABBREVIATIONS
BH = Bade Half
CCB — Continuing Calibration Blank
CCV » Continuing Calibration Verification
CHECK HS * Check High Standard
D = OUP = Anaiyticai DTpBnor (Piepared Dnpfrarr)
DA 3 Duplicate Analysis
FH = Front Half
FV = Enai Digestaie Volume
ICB = Imnai Calibration Blank
ICV = Tnirial Calibration Verification
ICSAB = Interference Check Solution (Solution AB)
       I = Tnirial
      Solution AB contains common inreifeiems in addition co the aoaiyte of interest.
DDL = Instrument Detection TJirrir
L = Serial Dilution
LCS = Liberator/ Control Spike Sample
NCB = Method Blank
MPV = Mercury Preparation Volume
MS = Prs-
-------
                 STANDARD CONCENTRATIONS
                for the TJA 61E TRACE ANALYZER
Analyte
Ag
As
AI
B
Ba
Be
Ca
Cd
Ce
Co
Cr
Cu
Fe
K
Li
Mg
Mn
Mo
Na
Ni
P
Pb
Sb
Se
Sn
Sr
Ti
Tl
V
Zn
Units
PpbM
ppb
ppb'-
ppb
ppb
ppb
ppb
ppb
ppb
ppb
ppb
ppb
ppb
ppb
ppb
ppb
ppb
ppb
ppb
ppb
ppb
ppb
ppb
ppb
ppb
ppb
ppb
ppb
Ppb
ppb
High Std
" 1 1000 <^;<
1000
"•"1000-*
1000
1000
1000
1000
1000
1000
1000
1000
1000
1000
10000
1000
1000
1000
1000
10000
1000
1000
1000
1000
1000
1000
1000
1000
1000
1000
1000
ICV/CCV
•v^sooV -
500
"'•"'t^&CAlV
£"„>.•;•' 3UU '
500
500
500
500
500
500
500
500
500
500
5000
500
500
500
500
5000
500
500
500
500
500
500
500
500
500
500
500
ICSAB
500 v
500
500000
500
500
500
500000
500
500
500
500
500
200000
19000
500
500000
500
500
5000
500
500
500
500
500
500
650
500
500
500
500
RDL
'-•1 -
5
:/;$o;
7
.2
1
60
1
3
1
2
2
40
220
1
30
2
2
300
3
30
2
4
3
13
1
8
5
2
12
Wavelength
3280
1890
3082
2496
4934
3130
3179
2265
4186
2286
2677
3247
2714
7664
6706
2790
2576
2020
3302
2316
2149
2203
2068
1960
1899
4215
3349
1908
2924
2062
Note: Use this reference page to review the raw data from the TJA 6IE Trace Analyzer.

This page includes the standard concentrations for the check high standard, initial calibration
verification (ICV), continuing calibration verification (CCV), and the interference check solution
(ICSAB).  In addition the reporting detection limit (RDL) and wavelength are reported for each
analyte.
                                                      Revision Date: 15-Jul-96
                                                                         11

-------
             CALCULATIONS FOR AIR SAMPLES

RESULTS FOR TRACE METALS (except mercury):

      RESULT in |ig (Front Half) = jig/L * FV CmU) * DF
                               1000 mL/L

     ^ RESULT in u,g (Back Half & Impingers) =  u.g/L * TV CmD * FV (mU) * DF
                                            mL used * 1000 mL/L

             FV = final volume in mL
             TV = total volume in mL
            . DF = Dilution Factor

The RESULTS for combined Front Half & Back Half samples use the same calculation as the
Back Half & impinger samples.

RESULTS FOR MERCURY (Kg):

       RESULT in u.g (Front Half) = ^ig/L * (mL FV/mL aliquot) * MPV * DF

       RESULT in jig (Back Half & Impingers) = ug/L * (mL TV/mL aliquot) * MPV * DF

             MPV = mercury preparation volume = 0.1 L

 %REC (Percent Recovery) for MS/MSP He spikes;

       %REC = spike sample results - original sample results * 100
                   true spike sample results

 NOTE: Original sample results less than the RDL are not used in calulations.

 %REC (Percent Recovery) for PDS:

        %REC = Spike sample ug/L cone. - original sample ug/L cone.  * 100
                         spike cone. (ug/L)

 %REC (Percent Recovery) for LCS/LCSD:

        %REC = SpDce sample u.g/L cone. * 100
                    spike cone. Qig/L)
  RPDs;       RPD =  I Result 2 - Result 1 I   * 100
                     (Result 2 + Result l)/2                          Rev. 2-Oct-96
                                                                          12

-------
Client:      Pacific Environmental Services
Project Number:        43411       	
 Sample Report
Client Sample ID:
TLI Sample ID:
Date Received'
Date Prepared:
Date Analyzed'
Matrix:
O-M29-1-FHACE,FHAR,FILTER FH
184-84-1 ABC FH
September 26. 1997
October 14-16. 1997
October 20. 1997
Air
Analyt& ;
Aa
As
Ba
Be
Cd
Co
Cr
Cu
Mn
Ni
P
Pb
Sb
Se
Tl
Zn















Cona
tooTU
2.411
-0.017
539.788
-0.158
-3.194
-32.448
125.993
71.253
677.158
59.056
505.792
30.749
38.440
46.739
1.600
214.073















mt
Total Vol.
N/A
N/A
N/A
N/A
N/A
N/A
N/A
N/A
N/A
N/A
N/A
N/A
N/A
N/A
N/A
N/A















mL
Used
N/A
N/A
N/A
N/A
N/A
N/A
N/A
N/A
N/A
N/A
N/A
N/A
N/A
N/A
N/A
N/A















mL
FtnalVol
100
100
100
100
100
100
100
100
100
100
100
100
100
100
100
100















Dilation
Factor
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1















Total ug. j
Result
0.241
< 0.500
54.0
< 0.100
< 0.100
< 0.100
12.6
7.13
67.7
5.91
50.6
3.07
3.84
4.67
< 0.200
21.4















Triangle Laboratories, Inc.
801 Capitola Drive * Durham, North Carolina 27713
Tele: (919) 544-5729 * Fax: (919) 544-5491
Printed:   Ol-Nov-97  at  03:09 PM
                                                                                  13

-------
Client:       Pacific Environmental Services
Project Number:	43411	
 Sample Report
Client Sample ID:
TLI Sample ID:
Date Received:
Date Prepared:
Date Analvzed:
Matrix:
O-M29-1-FHACEJFHAR.FILTER FH L
184-84-1 ABC FHL
September 26. 1997
October 14-16. 1997
October 20. 1997
Air
Analyte j
Aa
As
Ba
Be
Cd
Co
Cr
Cu
Mn
Ni
P
Pb
Sb
Se
Tl
Zn















Cone,
fcO/U
0.821
2.538
111.725
0.010
-0.554
-6.660
32.500
14.199
144.188
13.322
110.290
7.605
11.527
10.881
-0.400
46.879















mt
Total Voi
N/A
N/A
N/A
N/A
N/A
N/A
N/A
N/A
N/A
N/A
N/A
N/A
N/A
N/A
N/A
N/A















«t
Used
N/A
N/A
N/A
N/A
N/A
N/A
N/A
N/A
N/A
N/A
N/A
N/A
N/A
N/A
N/A
N/A















mt
Final Vot
100
100
100
100
100
100
100
100
100
100
100
100
100
100
100
100















Dilution
Factor
5
5
5
5
5
5
5
5
5
5
5
5
5
5
5
5















Total «Q '- ,
Result " -
< 0.500
< 2.50
55.9
< 0.500
< 0.500
< 0.500
16.3
7.10
72.1
6.66
55.1
3.80
5.76
5.44
< 1.00
23.4















Triangle Laboratories, Inc.
801 Capitola Drive * Durham, North Carolina 27713
Tele: (919) 544-5729 * Fax: (919) 544-5491
Printed:  Ol-Nov-97  at  03:09 PM
                                                                                  14

-------
 Client:      Pacific Environmental Services
 Project Number:	43411	
 Sample Report
Client Sample ID:
TLI Sample ID:
Date Received:
Date Prepared:
Date Analyzed'
Matrix:
O-M29-1-HNO3 BH
184-84-1DEBH
September 26. 1997
October 14-16. 1997
October 20. 1997
Air
Arialvte ;
Aa
As
Ba
Be
Cd
Co
Cr
Cu
Mn
Ni
P
Pb
Sb
Se
71
Zn















Core.
fcoto
1.302
-2.625
8.541
-0.012
4.544
-0.340
5.779
20.497
22.235
32.856
562.480
51.852
1.411
9.124
0.200
217.420















**,
TotatVol
1940
1940
1940
1940
1940
1940
1940
1940
1940
1940
1940
1940
1940
1940
1940
1940















ni.
Used
1840
1840
1840
1840
1840
1840
1840
1840
1840
1840
1840
1840
1840
1840
1840
1840















Rt
Final Vol.
100
100
100
100
100
100
100
100
100
100
100
100
100
100
100
100















Dlutfon
factor
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1















Total ug
Result j
0.137
< 0.527
0.901
< 0.105
0.479
< 0.105
0.609
2.16
2.34
3.46
59.3
5.47
< 0.422
0.962
< 0.21 1
22.9















Triangle Laboratories, Inc.
801 Capitola Drive * Durham, North Carolina 27713
Tele: (919) 544-5729 * Fax: (919) 544-5491
Printed:   Ol-Nov-97  at  03:09 PM
                                                                                 15

-------
Client:      Pacific Environmental Services
Project Number:	43411	
Sample Report
Client Sample ID:
TLI Sample ID:
Date Received:
Date Prepared:
Date Analvzed:
Matrix:
O-M29-1-HNO3 BH L
184-84-1DEBHL
September 26. 1997
October 14-16. 1997
October 20. 1997
Air
Analvte ;
Aa
As
Ba
Be
Cd
Co
Cr
Cu
Mn
Ni
P
Pb
Sb
Se
Tl
Zn















Cone.
fcoto
0.153
-2.144
1.564
-0.016
0.940
-0.489
1.401
3.143
3.694
5.411
108.558
11.312
0.320
0.079
0.500
44.302















" {&
ToferfVoL
1940
1940
1940
1940
1940
1940
1940
1940
1940
1940
1940
1940
1940
1940
1940
1940















Hi*
Used
1840
1840
1840
1840
1840
1840
1840
1840
1840
1840
1840
1840
1840
1840
1840
1840















nt
RnalVd.
100
100
100
100
100
100
100
100
100
100
100
100
100
100
100
100















Dilution
Factor
5
5
5
5
5
5
5
5
5
5
5
5
5
5
5
5















Totafuq
Result ;
< 0.527
< 2.64
< 1.05
< 0.527
< 0.527
< 0.527
< 1.05
1.66
1.95
2.85
57.2
5.96
< 2.11
< 1.58
< 1.05
23.4















Triangle Laboratories, Inc.
801 Capitola Drive * Durham, North Carolina 27713
Tele: (919) 544-5729 * Fax: (919) 544-5491
Printed:   Ol-Nov-97  at  03:09 PM
                                                                               16

-------
 Client:       Pacific Environmental Services
 Project Number;	43411	
 Sample Report
Client Sample ID:
TLI Sample ID:
Date Received:
Date Prepared:
Date Analvzed:
Matrix:
0-M29-2-FHACE J7HAR,FILTER FH
184-84-2ABC FH
September 26. 1997
October 14-16. 1997
October 20. 1997
Air
Analvte \
Aa
As
Ba
Be
Cd
Co
Cr
Cu
Mn
Ni
P
Pb
Sb
Se
Tl
Zn















Cone.
fcoto
2.154
2.119
401 .536
-0.235
1.741
-23.080
104.724
57.339
633.126
50.162
463.845
24.095
38.476
37.508
0.600
183.228















. mt
Total Vol.
N/A
N/A
N/A
N/A
N/A
N/A
N/A
N/A
N/A
N/A
N/A
N/A
N/A
N/A
N/A
N/A















, Bt
Used
N/A
N/A
N/A
N/A
N/A
N/A
N/A
N/A
N/A
N/A
N/A
N/A
N/A
N/A
N/A
N/A















mL
FaralVal
100
100
100
100
100
100
100
100
100
100
100
100
100
100
100
100















Difution
Factor
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1















Total w
Result
0.215
< 0.500
40.2
< 0.100
0.174
< 0.100
10.5
5.73
63.3
5.02
46.4
2.41
3.85
3.75
< 0.200
18.3















Triangle Laboratories, Inc.
801 Capitola Drive * Durham, North Carolina 27713
Tele: (919) 544-5729 * Fax: (919) 544-5491
Printed:  Ol-Nov-97  at   03:09 PM
                                                                             17

-------
 Client:      Pacific Environmental Services
 Project Number:	43411	
 Sample Report
Client Sample ED:
TLI Samole ID:
Date Received:
Date Prepared'
Date Analyzed:
Matrix:
O-M29-2-FHACE JHAR.FILTER FH DA
184-84-2ABCFHDA
Seotember26. 1997
October 14-16, 1997
October 20. 1997
Air
Analvte
Aa
As
Ba
Be
Cd
Co
Cr
Cu
Mn
Ni
P
Pb
Sb
Se
Tl
Zn















Cona
fco7L>
2.187
-2.546
401.409
-0.310
0.762
-25.496
104.896
58.095
630.072
50.148
444.771
21.354
32.953
39.887
N/A
181.032















mt
Total Vol.
N/A
N/A
N/A
N/A
N/A
N/A
N/A
N/A
N/A
N/A
N/A
N/A
N/A
N/A
N/A
N/A















Hit
Used
N/A
N/A
N/A
N/A
N/A
N/A
N/A
N/A
N/A
N/A
N/A
N/A
N/A
N/A
N/A
N/A















mt
RnalVof.
100
100
100
100
100
100
100
100
100
100
100
100
100
100
N/A
100















Dilution
Factor
1
1
1
1
1
1
1
1
1
1
1
1
1
1
N/A
1















Total w
Result
0.219
< 0.500
40.1
< 0.100
< 0.100
< 0.100
10.5
5.81
63.0
5.01
44.5
2.14
3.30
3.99
N/A
18.1















Triangle Laboratories, Inc.
801 Capitola Drive * Durham, North Carolina 27713
Tele: (919) 544-5729 * Fax: (919) 544-5491
Printed:  Ol-Nov-97  at  03:09 PM
                                                                              18

-------
 Client:       Pacific Environmental Services
 Project Number:        43411	
 Sample Report
Client Sample ID:
TLI Sample ID-
Date Received:
Date Prepared:
Date Analvzed:
Matrix:
O-M29-2-HN03 BH
184-84-2DE BH
Sentember26. 1997
October 14-16. 1997
October 20. 1997
Air
Aralvte
Aa
As
Ba
Be
Cd
Co
Cr
Cu
Mn
Ni
P
Pb
Sb
Se
Tl
Zn















Cone.
CUOTU
0.635
-3.373
7.088
-0.003
1.921
-0.164
5.627
13.779
110.581
14.447
660.558
28.585
0.257
6.474
0.800
73.430















*L
TdtfVoL
1910
1910
1910
1910
1910
1910
1910
1910
1910
1910
1910
1910
1910
1910
1910
1910















' rtiL
Used
1810
1810
1810
1810
1810
1810
1810
1810
1810
1810
1810
1810
1810
1810
1810
1810















nt
Final Vol.
100
100
100
100
100
100
100
100
100
100
100
100
100
100
100
100















•dutfon'
Factor
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1















TolalwQ
Result
< 0.106
< 0.528
- 0.748
< 0.106
0.203
< 0.106
0.594
1.45
11.7
1.52
69.7
3.02
< 0.422
0.683
< 0.211
7.75















Triangle Laboratories, Inc.
801 Capitola Drive * Durham, North Carolina 27713
Tele: (919) 544-5729 * Fax: (919) 544-5491
Printed:  Ol-Nov-97  at  03:09 PM
                                                                              19

-------
 Client:       Pacific Environmental Services
 Project Number:	43411	
 Sample Report
Client Sample ID:
TLI Samole ID-
Date Received:
Date Prepared:
Date Analyzed:
Matrix:
O-M29-2-HNO3 BH DA
184-84-2DEBHDA
September 26. 1997
October 14-16. 1997
October 20. 1997
Air
Analyte :
Aa
As
Ba
Be
Cd
Co
Cr
Cu
Mn
Ni
P
Pb
Sb
Se
Tl
Zn















Cona
tooto
-1.000
-2.338
6.838
-0.058
1.709
-1.009
4.196
12.233
109.478
13.690
650.906
28.606
-5.254
7.037
N/A
71.752















mL
TotatVol
1910
1910
1910
1910
1910
1910
1910
1910
1910
1910
1910
1910
1910
1910
N/A
1910















Hi.
* Used *
1810
1810
1810
1810
1810
1810
1810
1810
1810
1810
1810
1810
1810
1810
N/A
1810















nt
RnalVd.
100
100
100
100
100
100
100
100
100
100
100
100
100
100
N/A
100















D8utior>
Factor
1
1
1
1
1
1
1
1
1
1
1
1
1
1
N/A
1















Toteltjg i
Result
< 0.106
< 0.528
0.722
< 0.106
0.180
< 0.106
0.443
1.29
11.6
1.44
68.7
3.02
< 0.422
0.743
N/A
7.57















Triangle Laboratories, Inc.
801 Capitola Drive * Durham, North Carolina 27713
Tele: (919) 544-5729 * Fax: (919) 544-5491
Printed:  Ol-Nov-97  at   03:09 PM
                                                                                 20

-------
Client:       Pacific Environmental Services
Project Number:        43411      	
 Sample Report
Client Sample ID:
TLI Sample ID:
Date Received' —
Date Prepared:
Date Analyzed:
Matrix:
O-M29-3-FHACE.FHAR
FILTER FH
184-84-3 ABC FH
September 26. 1997
October 14-16. 1997
October 20. 1997
Air
Anah/te
Ad
As
Ba
Be
Cd
Co
Cr
Cu
Mn
Ni
P
Pb
Sb
Se
Tl
Zn















Cona
(UOto
0.873
3.733
692.085
-0.489
-1.272
-17.019
117.209
103.925
1075.564
63.151
762.477
31.982
39.115
39.481
-0.900
248.755















• mt
Total Vd.
N/A
N/A
N/A
N/A
N/A
N/A
N/A
N/A
N/A
N/A
N/A
N/A
N/A
N/A
N/A
N/A















3t
Used
N/A
N/A
N/A
N/A
N/A
N/A
N/A
N/A
N/A
N/A
N/A
N/A
N/A
N/A
N/A
N/A















ml
Final Vet
100
100
100
100
100
100
100
100
100
100
100
100
100
100
100
100















Dilation
Factor
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1















Total us
Result
< 0.100
< 0.500
69.2
< 0.100
< 0.100
< 0.100
11.7
10.4
108
6.32
76.2
3.20
3.91
3.95
< 0.200
24.9















Triangle Laboratories, Inc.
801 Capitola Drive * Durham, North Carolina 27713
Tele: (919) 544-5729 * Fax: (919) 544-5491
Printed:   Ol-Nov-97  at  03:09 PM
                                                                                21

-------
 Client:      Pacific Environmental Services
 Project Number:	43411	~
 Sample Report
Client Sample ID:
TLI Sample ID:
Date Received:
Date Prepared:
Date Analyzed"
Matrix:
0-M29-3-HNO3 BH
184-84-3DE BH
Seotember26. 1997
October 14-16. 1997
October 20. 1997
Air
	 ';
Analvte '
Aa
As
Ba
Be
Cd
Co
Cr
Cu
Mn
Ni
P
Pb
Sb
Se
Tl
Zn















C&na
'..tali
0.472
-4.540
6.268
-0.046
1.830
-1.202
8.405
42.971
77.676
16.960
645.299
26.987
0.675
9.011
0.900
73.823















rot
TotaJVol
1530
1530
1530
1530
1530
1530
1530
1530
1530
1530
1530
1530
1530
1530
1530
1530















JTi.
Used
1430
1430
1430
1430
1430
1430
1430
1430
1430
1430
1430
1430
1430
1430
1430
1430















, ni
Final VoL
100
100
100
100
100
100
100
100
100
100
100
100
100
100
100
100















Dilution
Factor
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1















Total tig
Result
< 0.107
< 0.535
0.671
< 0.107
0.196
< 0.107
0.899
4.60
8.31
1.81
69.0
2.89
< 0.428
0.964
< 0.214
7.90















Triangle Laboratories, Inc.
801 Capitola Drive * Durham, North Carolina 27713
Tele: (919) 544-5729 * Fax: (919) 544-5491
Printed:  Ol-Nov-97  at  03:09 PM
                                                                                22

-------
 Client:       Pacific Environmental Services
 Project Number:	43411	
 Sample Report
Client Sample ID:
TLI Samole ID-
Date Received:
Date Prepared:
Date Analyzed:
Matrix:
I-M29-1-FHACEFHARJFILTER FH
184-84-4 ABC FH
September 26. 1997
October 14-16. 1997
October 20. 1997
Air
Analyte
Aq
As
Ba
Be
Cd
Co
Cr
Cu
Mn
Ni
P
Pb
Sb
Se
Tl
Zn















Cona
femTU
11.971
50.286
10818.790
L -39.185
200.137
631.576
953.666
6107.147
24721 .447
574.107
42128.582
804.716
-2.931
-254.506
60.800
7400.913















0*, -
Total V
-------
Client:      Pacific Enyironmental Services
Project Number:	43411	
Sample Report
Client Sample ED:
TLI Sample DO:
Date Received:
Date Prepared:
Date Analyzed:
Matrix:
I-M29-1-HNO3 BH
184-84-4DBH
September 26. 1997
October 14-16. 1997
October 20. 1997
Air
Anatvte
Ad
As
Ba
Be
Cd
Co
Cr
Cu
Mn
Ni
P
Pb
Sb
Se
Tl
Zn















Oona I
tuofL\
-0.554
-5.631
4.733
-0.096
1.898
-1.351
3.620
13.739
12.341
13.553
345.681
41.442
-3.091
1.140
0.100
185.580















Fit
TotafVol -
750
750
750
750
750
750
750
750
750
750
750
750
750
750
750
750















' fit,
- 'U$«r '
650
650
650
650
650
650
650
650
650
650
650
650
650
650
650
650















TOL
FfoatVoI.
100
100
100
100
100
100
100
100
100
100
100
100
100
100
100
100















DiutioB
^Factor
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1















Tolalwg
Result
< 0.115
< 0.577
0.546
< 0.115
0.219
< 0.115
0.418
1.59
1.42
1.56
39.9
4.78
< 0.462
< 0.346
< 0.231
21.4















Triangle Laboratories, Inc.
801 Capitola Drive * Durham, North Carolina 27713
Tele: (919) 544-5729 * Fax: (919) 544-5491
Printed:   04-Nov-97  at  08:35 AM
                                                                                   24

-------
Client:       Pacific Environmental Services
Project Number:	43411	
 Sample Report
Client Sample ID:
TLI Sample ID-
Date Received:
Date Prepared:
Date Analyzed:
Matrix:
O-M29-FB .FHACE JHAR.2-FILTER 8/27/97 FH
184-84-5ABC FH
September 26. 1997
October 14-16. 1997
October 20. 1997
Air
^Analvte
Aa
As
Ba
Be
Cd
Co
Cr
Cu
Mn
Ni
P
Pb
Sb
Se
Tl
Zn















- Oona i
too« i
1.546
3.166
124.105
0.620
-4.483
-31 .070
106.758
46.528
377.059
48.807
289.196
-7.469
47.662
41.838
-0.600
101.157















rot
TotalVof,
N/A
N/A
N/A
N/A
N/A
N/A
N/A
N/A
N/A
N/A
N/A
N/A
N/A
N/A
N/A
N/A















8t
Used
N/A
N/A
N/A
N/A
N/A
N/A
N/A
N/A
N/A
N/A
N/A
N/A
N/A
N/A
N/A
N/A















0*.
FthalVof.
100
100
100
100
100
100
100
100
100
100
100
100
100
100
100
100















Dilution
Factor
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1















Total uq
Result
0.155
< 0.500
12.4
< 0.100
< 0.100
< 0.100
10.7
4.65
37.7
4.88
28.9
< 0.200
4.77
4.18
< 0.200
10.1















Triangle Laboratories, Inc.
801 Capitola Drive * Durham, North Carolina 27713
Tele: (919) 544-5729 * Fax: (919) 544-5491
Printed:  Ol-Nov-97  at  04:24 PM
                                                                                   25

-------
 Client:       Pacific Environmental Services
 Project Number:	43411	
 Sample Report
Client Sample ID:
TLI Sample ID:
Date Received'
Date Prepared:
Date Analvzed'
Matrix:
O-M29-FB-FHAR.HNO3 BH
184-84-5BD BH
September 26. 1997
October 14-16. 1997
October 20. 1997
Air
Analyte i
Aa
As
Ba
Be
Cd
Co
Cr
Cu
Mn
Ni
P
Pb
Sb
Se
Tl
Zn















Cona
fool*
2.048
-2.730
0.709
-0.041
0.216
-0.925
0.846
2.565
4.555
5.815
-10.251
3.934
0.598
-2.147
0.700
12.577















R*,
Total Vol
75
75
75
75
75
75
75
75
75
75
75
75
75
75
75
75















n»L
Used
75
75
75
75
75
75
75
75
75
75
75
75
75
75
75
75















: J*C
RnalVoi.
100
100
100
100
100
100
100
100
100
100
100
100
100
100
100
100















DSutton
Factor
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1















Totefug !
Result i
0.205
< 0.500
< 0.200
< 0.100
< 0.100
< 0.100
< 0.200
0.256
0.456
0.582
< 3.00
0.393
< 0.400
< 0.300
< 0.200
1.26















Triangle Laboratories, Inc.
801 Capitola Drive * Durham, North Carolina 27713
Tele: (919) 544-5729 * Fax: (919) 544-5491
Printed:  Ol-Nov-97  at  03:09 PM
                                                                          26

-------
 Client:       Pacific Environmental Services
 Project Number:	43411	
 Sample Report
Client Sample ED:
TLI Sample ID:
Date Received:
Date Prepared:
Date Analvzed:
Matrix:
I-M29-2-FHACE.FHAR JTLTER FH
184-84-6ABC FH
September 26. 1997
October 14-16, 1997
October 20. 1997
Air
Analvte ;
Aa
As
Ba
Be
Cd
Co
Cr
Cu
Mn
Ni
P
Pb
Sb
Se
Tl
Zn















Oona
fcote
10.016
38.155
9226.019
-18.610
142.849
550.989
872.942
6548.149
23324.377
555.005
38028.563
779.071
-25.276
-179.306
85.800
6658.945















mL
TotafVol
N/A
N/A
N/A
N/A
N/A
N/A
N/A
N/A
N/A
N/A
N/A
N/A
N/A
N/A
N/A
N/A















al
Used
N/A
N/A
N/A
N/A
N/A
N/A
N/A
N/A
N/A
N/A
N/A
N/A
N/A
N/A
N/A
N/A















mt
FinalVot
100
100
100
100
100
100
100
100
100
100
100
100
100
100
100
100















.. Dilution;
Factor
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1















Total us
Result
1.00
3.82
923
< 0.100
14.3
55.1
87.3
655
2330
55.5
3800
77.9
< 0.400
< 0.300
8.58
666















Triangle Laboratories, Inc.
801 Capitola Drive * Durham, North Carolina 27713
Tele: (919) 544-5729 * Fax: (919) 544-5491
Printed:   Ol-Nov-97  at  03:09 PM
                                                                           27

-------
Client:      Pacific Environmental Services
Project Number:	43411	
 Sample Report
Client Sample ID:
TLI Sample ID:
Date Received:
Date Prepared:
Date Analvzed:
Matrix:
I-M29-2-HNO3 BH
184-84-6DBH
September 26. 1997
October 14-16. 1997
October 20. 1997
Air
Anslvte
Ad
As
Ba
Be
Cd
Co
Cr
Cu
Mn
Ni
P
Pb
Sb
Se
Tl
Zn















Cona
Cuo/L}
0.446
-1.309
11.693
-0.062
3.081
0.488
9.077
48.382
52.124
26.162
667.446
46.649
-0.448
3.567
-0.200
150.872















. ML
Total VoL
1000
1000
1000
1000
1000
1000
1000
1000
1000
1000
1000
1000
1000
1000
1000
1000















rtL
Used
900
900
900
900
900
900
900
900
900
900
900
900
900
900
900
900















R*.
RnalVoi.
100
100
100
100
100
100
100
100
100
100
100
100
100
100
100
100















DSufor*
Factor
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1















Totefus i
Result
< 0.111
< 0.556
1.30
< 0.111
0.342
< 0.111
1.01
5.38
5.79
2.91
74.2
5.18
< 0.444
0.396
< 0.222
16.8















Triangle Laboratories, Inc.
801 Capitola Drive * Durham, North Carolina 27713
Tele: (919) 544-5729 * Fax: (919) 544-5491
Printed:  Ol-Nov-97  at  03:09 PM
                                                                              28

-------
Client:       Pacific Environmental Services
Project Number:         43411	
 Sample Report
Client Sample ID:
TLI Sample ID:
Date Received:
Date Prepared:
Date Analyzed :
Matrix:
I-M29-3-FHACE.FHAR.FILTER JH CATCH FH
184-84-7 ABCD FH
September 26. 1997
October 14-16, 1997
October 20. 1997
Air
Analvte :
Aa
As
Ba
Be
Cd
Co
Cr
Cu
Mn
Ni
P
Pb
Sb
Se
Tl
Zn















Oona
4wU
6.711
49.132
7308.835
-11.747
94.863
454.762
756.238
6031 .224
22375.820
463.733
48808.512
778.832
-1.819
-92.400
20.800
5198.991















mt
Total Vol.
N/A
N/A
N/A
N/A
N/A
N/A
N/A
N/A
N/A
N/A
N/A
N/A
N/A
N/A
N/A
N/A















'ml
Used
N/A
N/A
N/A
N/A
N/A
N/A
N/A
N/A
N/A
N/A
N/A
N/A
N/A
N/A
N/A
N/A















mt
FtnalVol
100
100
100
100
100
100
100
100
100
100
100
100
100
100
100
100















Ditutior*.
Factor
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1















Total us
Result
0.671
4.91
731
< 0.100
9.49
45.5
75.6
603
2240
46.4
4880
77.9
< 0.400
< 0.300
2.08
520















Triangle Laboratories, Inc.
801 Capitola Drive * Durham, North Carolina 27713
Tele: (919) 544-5729 * Fax: (919) 544-5491
Printed:  Ol-Nov-97  at  03:09 PM
                                                                              29

-------
Client:      Pacific Environmental Services
Project Number:	43411	
Sample Report
Client Sample ID:
TLI Sample ID:
Date Received:
Date Prepared:
Date Analvzed'
Matrix:
I-M29-3-HNO3 BH
184-84-7EFBH
September 26. 1997
October 14-16. 1997
October 20. 1997
Air
Analvte
Aa
As
Ba
Be
Cd
Co
Cr
Cu
Mn
Ni
P
Pb
Sb
Se
Tl
Zn















Cona
(tictfU
-0.107
-3.043
28.773
-0.035
2.943
0.034
11.196
38.729
95.115
35.373
1181.695
43.604
-0.121
0.198
0.000
298.429















fit.
. TotafVol
1100
1100
1100
1100
1100
1100
1100
1100
1100
1100
1100
1100
1100
1100
1100
1100















ni.
Used
1000
1000
1000
1000
1000
1000
1000
1000
1000
1000
1000
1000
1000
1000
1000
1000















f£
RnstVdL
100
100
100
100
100
100
100
100
100
100
100
100
100
100
100
100















Diu6on.
Factor
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1















Totefug \
Result
< 0.110
< 0.550
3.17
< 0.110
0.324
< 0.110
1.23
4.26
10.5
3.89
130
4.80
< 0.440
< 0.330
< 0.220
32.8















Triangle Laboratories, Inc.
801 Capitola Drive * Durham, North Carolina 27713
Tele: (919) 544-5729 * Fax: (919) 544-5491
Printed:  Ol-Nov-97  at   03:09 PM
                                                                              30

-------
Client:       Pacific Environmental Services
Project Number: 43411	
QA:  Serial Dilution
Client Sample ID:
TLI Sample ID:
Date Prepared:
Date Analyzed:
Matrix:
O-M29-1-FHACE,FHAR.FILTER FH
184-84-1ABC FH
October 14-16. 1997
October 20, 1997
Air
O-M29-1-FHACE.FHARJTLTER FH L
184-84-1 ABC FHL
October 14-16. 1997
October 20, 1997
Air

1 ' ;
Anahrte
Aq
As
Ba
Be
Cd
Co
Cr
Cu
Mn
Ni
P
Pb
Sb
Se
Tl
Zn















Native Sample
T<3ta|«9
Result
0.241
< 0.500
54.0
< 0.100
< 0.100
< 0.100
12.6
7.13
67.7
5.91
50.6
3.07
3.84
4.67
< 0.200
214















ugl
	 Cone. 	
2.411
-0.017
539.788
-0.158
-3.194
-32.448
125.993
71.253
677.158
59.056
505.792
30.749
38.440
46.739
1.600
214.073















Serial Dilution
Tobl«9 ' % ' :
	 Result 	
< 0.500
< 2.50
55.9
< 0.500
< 0.500
< 0.500
163
7.10
72.1
6.66
55.1
3.80
5.76
5.44
< 1.00
234















«#• i
	 Cone... ..
0.821
2.538
111.725
0.010
-0.554
-6.660
32.500
14.199
144.188
13.322
110.290
7.605
11.527
10.881
-0.400
46879















ffff
m*-

-------
Client:      Pacific Environmental Services
Project Number: 43411	
QA:  Serial Dilution
Client Sample ID:
TLI Sample ID'
Date Prepared:
Date Analyzed:
Matrix:
O-M29-1-HNO3 BH
184-84-1DEBH
October 14-16. 1997
October 20. 1997
Air
O-M29-1-HNO3BHT.
184-84-1DE BH L
October 14-16. 1997
October 20. 1997
Air

AnaMe
Aq
As
Ba
Be
Cd
Co
Cr
Cu
Mn
Ni
P
Pb
Sb
Se
Tl
Zn















Native Sample
Total ug
Result
0.137
< 0.527
0.901
< 0.105
0.479
< 0.105
0.609
2.16
2.34
3.46
59.3
5.47
< 0.422
0.962
< 0.211
22.9















ygl
Cone.
1.302
-2.625
8.541
-0.012
4.544
-0.340
5.779
20.497
22.235
32.856
562.480
51.852
1411
9.124
0.200
217.420















Serial Dilution
Toted &g
Resut
< 0.527
< 2.64
< 1.05
< 0.527
< 0.527
< 0.527
< 1.05
1.66
1.95
2.85
57.2
5.96
< 2.11
< 1 58
< 105
234















<#t i
Cone* \
0.153
-2.144
1.564
-0.016
0.940
-0.489
1.401
3.143
3.694
5.411
108.558
11.312
0320
0079
0500
44.302















RPD

-------
Client:           Pacific Environmental Services
Project Number;	43411
QA:  Duplicate
Client Sample ID-
TLI Sample ID:
Date Prepared:
Date Analyzed:
Matrix:
O-M29-2-FHACE.FHAR.FILTER FH
184-84-2ABC FH
October 14-16. 1997
October 20. 1997
Air
O-M29-2-FHACRFHAR.FILTER FH DA
184-84-2ABCFHDA
October 14-16. 1997
October 20. 1997
Air

Analyte
Aa
As
Ba
Be
Cd
Co
Cr
Cu
Mn
Ni
P
Pb
Sb
Se
Tl
Zn















Sample
Total a
-------
Client:         Pacific Environmental Services
Project Number:	43411
QA: Duplicate
Client Sample ID:
TLI Sample ID:
Date Prepared:
Date Analyzed:
Matrix:
O-M29-2-HNO3 BH
184-84-2DE BH
October 14-16. 1997
October 20. 1997
Air
0-M29-2-HNO3BHDA
184-84-2DEBHDA
October 14-16. 1997
October 20. 1997
Air

Anatvte
Aq
As
Ba
Be
Cd
Co
Cr
Cu
Mn
Ni
P
Pb
Sb
Se
Tl
Zn















Sample
" Totelug i
•' Result i
< 0.106
< 0.528
0.748
< 0.106
0.203
< 0.106
0.594
1.45
11.7
1.52
69.7
3.02
< 0.422
0.683
< 0.211
7.75















wg/L,
Cone*'
0.635
-3.373
7.088
-0.003
1.921
-0.164
5.627
13.779
110.581
14.447
660.558
28.585
0.257
6.474
0.800
73.430















Duplicate
', Ttfteiagi - -.
Resuft
< 0.106
< 0.528
0.722
< 0.106
0.18
< 0.106
0.443
1.29
11.6
1.44
68.7
3.02
< 0.422
0.743
N/A
757















I*. i
Core.
-1.000
-2.338
6.838
-0.058
1.709
-1.009
4.196
12.233
109.478
13.690
650.906
28.606
-5.254
7.037
N/A
71 752















BPfc

-------
Client:  Pacific Environmental Services
Project Number:      43411
QA: Matrix Spikes (Post-Digestion)
Client Sample ID:
TLI Sample ID-
Date Prepared:
Date Analyzed:
Matrix'
O-M29-1-FHACE.FHAR.RL7ER FH PDS
184-84-1 ABC FHPDS
October 14-16, 1997
October 20. 1997
Air






Anaivte
Aq
As
Ba
Be
Cd
Co
Cr
Cu
Mn
Ni
P
Pb
Sb
Se
Tl
Zn















Post-Die
f:teewer«t
Amount {tiflfl-V
42.33
47.28
575.52
44.63
43.53
17.32
172.26
118.97
709.59
105.88
1391.02
75.53
95.35
85.76
20.40
397.21















estton Spike
Spjke -
Amount fooft-V
50
50
50
50
50
50
50
50
50
50
1000
50
50
50
25
200















- %
Recovery
80°/<
95°/c
Spike Low
89°/<
87°/<
35°/<
93°/c
95°/c
Spike Low
94°/<
89°/<
90°/<
114°/<
78°/<
82°/<
92°/
-------
Client:   Pacific Environmental Services
Project Number:	43411	
QA: Matrix Spikes (Post-Digestion)
Client Sample ID:
Tl.T Sample TD:
Date Preoared:
Date Analyzed:
Matrix:
O-M29-1-HN03BHPDS
184-84-1DEBHPDS
October 14-16. 1997
October 20. 1997
Air






.Analyie,,,
Aa
As
Ba
Be
Cd
Co
Cr
Cu
Mn
Ni
P
Pb
Sb
Se
Tl
Zn















Post-Die
BBttffBmt
Amount ftjoO
42.65
42.89
58.97
46.31
51.82
47.41
52.63
68.63
63.17
79.71
1419.02
96.36
45.56
50.52
21.90
389.40















estton Spike
Sp»K*
Amount fuafLV "
50
50
50
50
50
50
50
50
50
50
1000
50
50
50
25
200















• * %,
Reeoverv
83°/<
86°/<
101°X
93°/<
95°/<
95°/<
947«
96°/<
82°X
94°X
8&K
89°/<
91 "A
83°/
88°/<
86°/















Post-Digestion Spike Duplicate
Repftgrad i
£nx»MftjaO;































^ Sp&e •
,Amo«Tt&ra&3































* -*
Recovery































V
' ;tm
*. .jA,
Igft-t f


»*—
»-
...
...
...
...
—
...
...

...
...


...
...
— —
...
...
...

.«
...
...

...
..


Triangle Laboratories, Inc.
801 Capitola Drive * Durham, NC 27713
Tele: (919) 544-5729 * Fax: (919) 544-5491
Printed:    Ol-Nov-97
at
04:24 PM
                                                                                           36

-------
Client:   Pacific Environmental Services
Project Number:   43411	
QA: Method Blank
TLI Sample ID:
Date Prepared'
Date Analyzed:
Matrix:
4141 1 MB
October 14-16. 1997
October 20. 1997
N/A

' AnaMe
Aa
As
Ba
Be
Cd
Co
Cr
Cu
Mn
Ni
P
Pb
Sb
Se
Tl
Zn















Method Blank
Recovered
Amount fad/O
-0.31
-0.83
0.08
-0.01
0.03
-0.32
0.26
0.73
0.39
10.14
-5.19
0.71
-0.06
0.50
-1.30
2.79















Detection
UmiUuo/l}
1
5
2
1
1
1
2
2
2
3
30
2
4
3
2
12
—
—
—
—
—
—
—
—
—
—
—
—
—
—
...

Pass or
Fail
Pass
Pass
Pass
Pass
Pass
Pass
Pass
Pass
Pass
Fail
Pass
Pass
Pass
Pass
Pass
Pass
...
...
—
...
...
...
...
—
—

...
—
—
—
—
Triangle Laboratories, Inc.
801 Capitola Drive * Durham, NC 27713
Tele: (919) 544-5729 * Fax: (919) 544-5491
Printed:  Ol-Nov-97
                      at
03:11 PM
                                                                           37

-------
Client:  Pacific Environmental Services
Project Number:	43411	
QA: Lab Control Spikes
TLT Sample TD:
Date Prepared:
Date Analyzed:
Matrix:
43411 LCS
October 14-16.1997
October 20. 1997
N/A

Analvte
Ag
As
Ba
Be
Cd
Co
Cr
Cu
Mn
Ni
P
Pb
Sb
Se
Tl
Zn















Lab Control Spike
iteo^K**
Amount &ofl_>
42.95
44.95
46.80
45.78
46.59
46.65
47.19
47.89
47.50
65.43
908.82
45.94
46.51
46.39
36.40
194.41















Spite --;
Amount luafti '.''...
50
50
50
50
50
50
50
50
50
50
1000
50
50
50
50
200















}*&%,,
Recover*
86°X
90°/<
94°/<
92°/<
93°/<
93°/<
94°/<
96°/<
957<
131°/<
91°/<
927<
93°/<
93°/<
73°/<
97°/<















Lab Control Spike Duplicate
BecQvered ;
Amount t uq/L\:































$&»^ f,
Anxjont CuoA.^































%--,
Recovery































TO
._
...
—
	
...
—
...
—
...

...
».

_„
...
...
...
	
...
...
—
...
...
—
—
	
	
—
...
...
—
 Triangle Laboratories, Inc.
 801 Capitola Drive * Durham, NC 27713
 Tele: (919) 544-5729 * Fax: (919) 544-5491
                                      Printed:   Ol-Nov-97
at
03:11 PM
                                                                                      38

-------
 Client:      Pacific Environmental Services
 Project Number:	43377	
 Sample Report
Client Sample ED:
TLI Samole ID:
Date Received'
Date Preoared:
Date Analyzed:
Matrix:
O-M29-RB-FHACEJ3HARJTLTER FH
184-50-6ABC FH
September 24 1997
October 10-14. 1997
October 16.20 21 & 22. 1997
Air
•, •»*• •"
; 'A ..A-^A
: Analyte^ *
Aa
As
Ba
Be
Cd
Co
Cr
Cu
Mn
Ni
P
Pb
Sb
Se
•n
Zn
















2.705
3.407
43292
-0.112
•6.215
-29.571
93294
10.580
9.109
46.803
17.600
-12.883
41.765
43.531
-3.00
25.989
















N/A
N/A
N/A
N/A
N/A
N/A
N/A
N/A
N/A
N/A
N/A
N/A
N/A
N/A
N/A
N/A















jv; -«(.»,!
; ~ Utodk* ;
N/A
N/A
N/A
N/A
N/A
N/A
N/A
N/A
N/A
N/A
N/A
N/A
N/A
N/A
N/A
N/A















'c"*«iL* J
Final Vdb \
100
100
100
100
100
100
100
100
100
100
100
100
100
100
100
100















iPlfe
5Sij&j/f?f v' ^v*
^j\ ^ToSSKftv **
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
















0270
< 0.500
4.33
< 0.100
< 0.100
< 0.100
9.33
1.06
0.911
4.68
< 3.00
< OJ200
4.18
4.35
< 0.200
2.60















Triangle Laboratories, Inc.
801 Capitola Drive * Durbam, North Carolina 27713
Tele: (919) 544-5729 * Fax: (919) 544-5491
Printed:  03-Nov-97  at   01:08 PM

-------
Client:       Pacific Environmental Services
Project Number;	43377	
 Sample Report
Client Sample ID:
TLI Samole ID:
Date Received'
Date Preoafed:
Date Analyzed'
Matrix:
O-M29-RB-HN03 BH
184-50-6BDBH
September 24. 1997
October 10-14. 1997
October 16.20.21 & 22, 1997
Air
Analvte ^ !
Aa
As
Ba
Be
Cd
Co
Cr
Cu
Mn
Ni
P
Pb
Sb
Se
Tl
Zn















P*N1
0.061
-8.994
3.256
-0.044
-0.536
-1.619
£217
14.381
346.891
6.056
553.359
2647
1.642
•0.017
-1.50
20.330















%&- ISL JL \
i¥
-------
lient:
•oiect Number:
Pacific Environmental Services
 	43411
ample Report
                           Page 1 of 4
te Received:
te Prepared :
te Analv7ed"
,TA FILE:
trix:
Ser»ember 26. 1997
October 14-20. 1997
October 20-22. 1997
AB826 AB827&AB828
Air
                                                                                 ANALYT& Ho
                                                                                 uo/LRDL: O.2
                                                                                 Analvsis Method*
                                                                                                    29
                                                                                 Instrument P E Teaman 5100
                                                                                 Soike Cone. (uq/U     5
                                                 CVAA ANALYTE SUMMARY REPORT
H-ffSarnoteKi' •• ' ;
M29-1-FHACE,FHAR,FILTER FH
M29-1-FHACE,FHAR,FILTER FH D
M29-1-HNO3BH
M29-1-HNO3BHD
M29-1-BHARHNO3
M29-1-BHARHN03D
M29-1-KMnO4
M29-1-KMnO4D
M29-1-HCI
M29-1-HCID
M29-2-FHACE,FHAR,FILTER FH
M29-2-FHACE,FHAR,FILTER FH D
V129-2-HNO3BH
VI29-2-HN03 BH D
VI29-2-BHAR HNO3
V129-2-BHAR HNO3 D
v129-2-KMnO4
v129-2-KMn04 D
d29-2-HCI
^29-2-HCI D
d29-3-FHACE,FHAR,FILTER FH
J29-3-FHACE,FHAR,FILTER FH D
JI29-3-HNO3 BH
/I29-3-HNO3 BH D
/129-3-BHAR HNO3
/129^-BHAR HNO3 D
d29-3-KMnO4
te9-3-KMnO4 D
129-3-HCI
129-3-HCI D
TUSAMPID
184-84-1ABC
184-84-1 ABC D
1 84-84-1 DE
1 84-84-1 DED
1 84-84-1 F
t84-84-lFD
1 84-84-1 G
1 84-84-1 G D
1 84-84-1 H
1 84-84-1 HD
184-84-2ABC
184-84-2ABCD
184-84-2DE
184-84-2DED
184-84-2F
184-84-2FD
184-84-2G
184-84-2GD
184-84-2H
184-84-2HD
184-84-3ABC
184-84-3ABCD
184-84-3DE
184-84-3DED
184-84-3F
184-84-3FD
184-84-3G
184-84-3G D
184-84-3H
184-84-3H D
UOtXi
CONG-'
0.022
0.006
0.016
0.020
0.019
0.012
0.070
0.072
0.011
0.002
0.006
-0.002
0.019
0.019
0.000
0.000
0.033
0.093
0.019
0.014
0.009
0.008
0.025
0.014
0.012
0.006
0.107
0.106
0.016
0.019
-M
IV
N/A
N/A
1940
1940
110
110
450
450
89
89
N/A
N/A
1910
1910
90
90
455
455
46
46
N/A
N/A
1530
1530
85
85
265
265
50
50
rat
FV-
100
100
N/A
N/A
N/A
N/A
N/A
N/A
N/A
N/A
100
100
N/A
N/A
N/A
N/A
N/A
N/A
N/A
N/A
100
100
N/A
N/A
N/A
N/A
N/A
N/A
N/A
N/A
mi
Afiquol
5
5
5
5
5
5
5
5
5
5
5
5
5
5
5
5
5
5
5
5
5
5
5
5
5
5
5
5
5
5
OIL
FACTQF
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
Totatuo
RESUL1
< 0.400
< 0.400
< 7.76
< 7.76
< 0.440
< 0.440
< 1.80
< 1.80
< 0.356
< 0.356
< 0.400
< 0.400
< 7.64
< 7.64
< 0.360
< 0.360
< 1.82
< 1.82
< 0.184
< 0.184
< 0.400
< 0.400
< 6.12
< 6.12
< 0.340
< 0.340
< 1.06
< 1.06
< 0.200
< 0200
,'•: -vAYCt ssj
- *FE5ULTi
< 0.400
< 7.76
< 0.440
< 1.80
< 0.356
< 0.400
< 7.64
< 0.360
< 1.82
< 0.184
< 0.400
< 6.12
< 0.340
< 1.06
< 0.200
"8 v..
"BPD.
-
_
—
_
-
-
_
-
-
_
-
-
-
-
-
*&iic:
_
_
_
_
_
-
_
— .
-
-
_
	
	
-
-
                                                                                                     39

-------
Client: Pacific Environmental Services
Project Number: 43411
Sample Report
Date Received:
Date Prepared :
Date Analyzed:
DATA FILE:
Matrix:
September 26. 1997
October 14-20. 1997
October 20-22. 1997
AB826, AB827 & AB828
Air
Page 2 of 4

ANALYTE: Ha
ua/L RDL 0.2
AnSlVSJS Method1 29
Instrument P E Zeeman 5100
SoikeConc (uo/U S
-
CVAA ANALYTE SUMMARY REPORT

I-M29-1-FHACE,FHAR,FILTER FH
I-M29-1-FHACE,FHAR,FILTER FH D
I-M29-1-HNO3 BH
rl-M29-1-HNO3BHD
l-M29-1-KMnO4
l-M29-1-KMnO4D
I-M29-1-HCI
I-M29-1-HCID
O-M29-FB-FHACE,FHAR,2-FILTER 8/27/97 FH
O-M29-FB-FHACE.FHAR.2-FILTER 8/27/97 FH D
0-M29-FB-FHAR.HNO3 BH
O-M29-FB-FHAR.HNO3 BH D
O-M29-FB-BHAR HNO3
O-M29-FB-BHAR HNO3 D
O-M29-FB-KMnO4
O-M29-FB-KMn04 D
O-M29-FB-HCI
O-M29-FB-HCI D
l-M29-2-FHACE,FHAR,FILTER FH
l-M29-2-FHACE,FHAR,FILTER FH D
I-M29-2-HNO3 BH
I-M29-2-HNO3 BH D
I-M29-2-BHAR HNO3
I-M29-2-BHAR HNO3 D
l-M29-2-KMnO4
l-M29-2-KMnO4 D
I-M29-2-HCI
I-M29-2-HCI D
ti.SAMttO^ ^
184-84-4ABC
184-84-4ABC D
184-84-4D
184-84-4DD
184-84-4E
184-84^E D
184-84-4F
184-64-4FD
184-84-5ABC
184-84-5 ABC D
184-84-5BD
184-84-5BDD
184-84-5E
184-84-5E D
184-84-5F
184-84-5FD
184-84-5GF
184-84-5GFD
184-84-6ABC
184-84-6 ABC D
184-84-6D
184-84-6D D
184-84-6G
184-84-6G.P.', '. .
184-84-6E
184-84-6ED
184-84-6F*... -.- •- v
184-84-6FO'
ffffe
0.059
0.062
0.026
0X116
0.081
0.048
0.011
0.012
0.005
0.002
0.050
0.033
a041
0.036
0.030
0.025
O044
O041
0X81
0X178
0.044
0.039
O034
•aoaa
ai38
0.127
•0.003
0,003
W
N/A
N/A
750
750
33S
335
49
49
WA
N/A
*7S
* 75
75
75
400
400
SO
50
N/A
MM
1000
1000
75
75
300
300
63
63
**$
100
100
N/A
N/A
MM
N/A
N/A
N/A
TOO
too
N/A
N/A
N/A
N/A
N/A
N/A
NCA
N/A
100
100
N/A
N/A
N/A
N/A
N/A
N/A
N/A
N/A
* *!*"
5
5
5
5
5
5
5
5
5
5
5
S
5
5
5
5
5
5
5
5
5
5
5
5
5
5
5
5
DJL
1
1
1
1 "
1
1
1
1
1
1
1
1
1
1
1 ,
1
1
1
1
1
1
1
1
1
1
1
1
1
>, TateftM
< 0.400
< 0.400
< 3.00
< 3.00
< 1.34
< 1.34
< 0.196
< 0.196
< 0*400
< O400
< O300
< 0.300
< 0.300
< 0.300
< 1.60
< 1.60
< 0200
< 0200
< 0.400
< 0,400
•-• " 4.00
< 4.00
< 0.300
< 0.300
< 120
< 120
< 0.252
< 0252
,-."- Ava ¥«*

< 0.400
_
< 3.00

< 1.34

< 0.196

< 0.400

< 0300

< 0.300

< 1.60

< 0200
_
< 0,400

< 4.00

< Ob300

< 120

< 0252


-

-

-

-

-

-

-

-

-
_
-

-

-

-

-


-

-

-

-

-

-

•-

-

-

-

-

-

-

-
                                      40

-------
lent:
oiect Number;
Pacific Environmental Services
       	43411
ample Report
                         Page 3 of 4
: Received:
s Preoared:
' Analyzed:
FA FILE:
nx:
September 26. 1997
October 14-20. 1997
October 20-22. 1997
AB826, AB827 A AB828
Air
ANALYTE: Ha
ua/L RDL 02
Analysis Method:
29
Instrument P E Zeeman 5100
Soike Cone. (ua/L)
5
                                             CVAA ANALYTE SUMMARY REPORT
* " " - ,l
•rtSaitttetD '" - ]
29-3-FHACE,FHAR,FILTER,FH CATCH FH
29-3-FHACE,FHAR,FILTER,FH CATCH FH D
29-3-HNO3 BH
29-3-HNO3 BH D
29-3-BHAR HNO3
29-3-BHAR HNO3 D
29-3-KMnO4
29-3-KMnO4 D
29-3-HCI
29-3-HCI D
129-1 -HNO3BH MS
129-1 -HNO3BHMSD
129-2-HNO3 BH MS
129-2-HNO3 BH MSD
29-1-HNO3BHMS
S-1-HNO3BHMSD
I29-FB-FHAR.HNO3 BH MS
I29-FB-FHAR,HNO3 BH MSD
S-2-HNO3 BH MS
I9-2-HNO3 BH MSD
9-3-HNO3 BH MS
I9-3-HNO3 BH MSD
29-1-HNO3BHMS
29-1 -HNO3BH MSD
29-2-HNO3 BH MS
29-2-HNO3 BH MSD
9-1-HNO3BHMS
9-1-HNO3BHMSD
29-FB-FHAR,HNO3 BH MS
»-FB-FHAR,HN03 BH MSD
3-2-HNO3 BH MS
9-2-HNO3 BH MSD
	 "•;
TtlSAl«PlD
84-64-7ABCD
84-84-7ABCD D
184-84-7EF
184-84-7EFD
184-84-7G
184-64-7GD
184-84-7H
184-84-7H D
184-84-7H
184-64-7H D
184-84-1 DEMS
1 84-84-1 DE MSD
184-84-2DEMS
184-84-2DE MSD
184-84-4DMS
184-84-4DMSD
184-64-5BDMS
184-84-5BDMSD
184-84-60 MS
184-84-6DMSD
184-84-7EFMS
184-84-7EFMSD
True Spike MS
True Spike MSD
True Spike MS
True Spike MSD
Tiue Spike MS
True Spike MSD
True Spike MS
True Spike MSD
True Spike MS
True Spike MSD
uatL
OJNfc
0.031
0.018
0.044
0.036
0.000
•0.018
0.148
0.112
0.148
0.112
2.521
2.532
£922
2.720
2.599
£631
4.926
5.092
8.142
7.947
8.442
8.587
5
5
5
5
5
5
5
5
5
c
ml
TV
N/A
N/A
1100
1100
105
105
235
235
100
100
1940
1940
1910
1910
750
750
75
75
1000
1000
1100
1100
1940
1940
1910
1910
750
750
75
75
1000
1000
8*
fV
100
100
N/A
N/A
N/A
N/A
N/A
N/A
N/A
N/A
N/A
N/A
N/A
N/A
N/A
N/A
N/A
N/A
N/A
N/A
N/A
N/A
N/A
N/A
N/A
N/A
N/A
N/A
N/A
N/A
N/A
N/A
^wt .
A&ttJdf
5
5
5
5
5
5
5
5
5
5
5
5
5
5
5
5
5
5
5
5
5
5
5
5
5
5
5
5
5
5
5
5
m< ,
ftWSSK*
1
1
1
1 -
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
Totelw
'ftS&JLt
< 0.400
< 0.400
< 4.40
< 4.40
< 0.420
< 0.420
< 0.940
< 0.940
< 0.400
< 0.400
98
98
112
104
39.0
39.5
7.39
7.64
163
159
186
189
194
194
191
191
75.0
75.0
7.50
7.50
100
100
"" y" ASHXV'"-
-aestiLf
_
< 0.400
_
< 4.40
_
< 0.420
_
< 0.940
_
< 0.400

98
__
1O8
_
39.2
_
7.51
_
161
_
187
_
-
_
-
__
-
^
-
_
—
,-W-V
RPDf
_
-
__
-
_
-
—
-
_
—

0.44%
—
7.16%
_
122%
_
3.31%
_
2.42%
„,
1.70%
__
-
_
-
_
-
_
-
_
-
^V^ < *,' :
^66
_
-
_
-
._
-
*.
-
__
—
50%
51%
58%
54%
52%
53%
99%
102%
163%
159%
169%
172%
	
-
..
-

-

-

—
                                                                                          41

-------
Client:
Project Number:
 Pacific Environmental Services
	43411
Sample Report
                              Page 4 o«4
Date Received:
Date Prepared:
Date Analv7edi
DATA FILE:
Matrix:
.September 26 1997
October 14-20. 1997
October 20- 22 1997
AB826. AB827 & AB828
Air
                                                                                         ANALYTF- Ho
                                                                                         uo/L RDL:  0.2
                                                                                         Analuaig Method-
                                                                                         Instrument P E Zeeman 5100
                                                                                         Soite Cone. kio/L\     5
                                                       CVAA ANALYTE SUMMARY REPORT
CSentSartpteJOt :
I-M29-3-HNO3 BH MS
I-M29-3-HNO3 BH MSD
Method Blank
Method Blank D
LCS
LCSD
Method Blank
Method Blank D
LCS
LCSD
Method Blank
Method Blank D
LCS
LCSD
TLfSAMPID
True Spike MS
True Spike MSD
43411 MB1
43411 MB01
43411 LCS1
43411 LCS1D
4341 1MB2
4341 1 MBD2
43411 LCS2
43411 LCS2D
4341 1 MB3
43411 MBD3
43411LCS3
43411 LCS3D
*©t-
CONC;
5
5
0.006
OOQB
5.006
4.900
0.005
-Q.01O
5.325
&473
0.036
0.022
5.001
4.846
-Irt
W
1100
1100
—
-
—
—
-
-
nrt
FV
N/A
N/A
-
-
_
_
^ »
-
ml
5
5
;
-
_
-
_
-
, OIL
FACTOT
1
1
-
-
„
_
j_
- -
,;::Ta*atutt
^S0L!
110
110
-
-
_
-
-
-
Avet,:
RESULT:
-
-
-
_
«•
- :
-
&F®

-
_
:
,
-
-
i4Rga1

-
100%
98%
-
107%
109%
-
100%
97%
Triangle Laboratories, Inc.
801 Capitola Drive * Durham, North Carolina 27713
Tele: (919) 544-5729 * Fax: (919) 544-5491
                                                   Printed:    01-No*07
                                                                             0320PM
                                                                                                                     r»

-------
O PACIFIC ENVIRONMENTAL SERVICES. INC.
\ff      wuu i wuuin iviianii uuuicvcinj, r.^J. DOX
   Research Triangle Park, North Carolina 27709-2077'
              (919) 941-0333 FAX: (919) 941-0234
                                                    Chain of Custody Record
Project Num
s4 13-004
Project Name AO*HH -RA*ST"R''
US EPA EMC Asphalt Cement,
Samplers:
Dickerson, McDonald, Thompson, Dougherty, Hamilton
Date
8/27/97
8/27/97
8/27/97
8/27/97
8/27/97
8/27/97
8/27/97
8/27/97
8/28/97
8/28/97
8/28/97
8/28/97
8/28/97
8/28/97
8/28/97
8/28/97
8/29/97
8/29/97
8/29/97
8/29/97
8/29/97
8/29/97
8/29/97
8/29/97
8/27/97
i
Time
1600
1600
1600
1600
1600
1600
1600
1600
1300
1300
1300
1300
1300
1300
1300
1300
1315
1315
1315
131(5
13,15
13^5
131.5
1315
1300
Field Sample ID
O-M29-1-FHACE
O-M29-1-FHAR
O-M29-1 -Filter
O-M29-1-HNO3
O-M29-1-HNO4
O-M29-1-BHAR
O-M29-1-KMnO4
O-M29-1-HCI
O-M29-2-FHACE
O-M29-2-FHAR
O-M29-2-Filter
O-M29-2-HNO3
O-M29-2-HNO3
O-M29-2-BHAR
O-M29-2-KMnO4
O-M29-2-HCI
O-M29-3-FHACE
O-M29-3-FHAR
O-M29-3-Filter
O-M29-3-HNO3
O-M29-3-HNO3
O-M29-3-BHAR
O-M29-3-KMnO4
O-M29-3-HCI
-M29-1-FHACE
Sample Description
FH Acetone Rinse - Beaker No. M-22
FH0.1 NHNO3 Rinse
Filter M97-013 - Beaker No. M-23
5% HNO3 / 10% H2O2 Absorbing Solution
5% HNO3 / 10% H2O2 Absorbing Solution
BH 0.1 N HN03 Rinse
10.% H2SO4 / 4% KMnO4 Absorbing Sol.
8N HCI Rinse
FH Acetone Rinse - Beaker No. M-24
FH0.1 NHNO3 Rinse
Filter M97-0 19
5% HNO3 / 10% H2O2 Absorbing Solution
5% HNO3 / 10% H2O2 Absorbing Solution
BH0.1 NHNO3 Rinse
10% H2SO4 /4% KMnO4 Absorbing Sol.
8N HCI Rinse
FH Acetone Rinse - Beaker No. W-10
FH0.1 NHNO3 Rinse
Filter M97-004 - Beaker No. W-1 1
5% HNO3 / 10% H2O2 Absorbing Solution
5% HNO3 / 10% H2O2 Absorbing Solution
BH0.1 NHN03 Rinse
10% H2S04 / 4% KMnO4 Absorbing Sol.
8N HCI Rinse
FH Acetone Rinse - Beaker No. M-12
Analysis Requested
MM
•
.
•
.
*
.


.
•
*
•
.
.


*
.
.
.
.
•


•
Hg
•
.
.
.
.
.
.
.
.
.
.
.
.
.
.
. .
.
.
.
t
.
.
.
.
•










































i
























































































Remarks



Bottle 1/2
Bottle 2/2





Petri Disk
Bottle 1/2
Bottle 2/2





Bottle 1/2
Bottle 2/2 '




                                                           Page 1 of 3

-------
O PACIFIC ENVIRONMENTAL SERVICES. INC.
                          Central Park West
     5001 South Miami Boulevard, P.O. Box 12077.
Research Triangle Park, North Carolina 27709-2077
           (919) 941-0333 FAX: (919) 941-0234
                                                   Chain of Custody Record
*








a


S413-004

Project Name jo****- Xstrtr^
US EPA EMC Asphalt Cement, *
Samplers: ,
Dickerson, McDonald, Thompson. Dougherty, Hamilton
Date
8/27/97
8/27/97
8/27/97
. 8/27/97
8/27/97
8/27/97
8/27/97
8/27/97
8/27/97
8/27/97
8/27/97
8/27/97
8/28/97
8/28/97
8/28/97
8/28/97
8/28/97
8/28/97
8/29/97
8/29/97
8/29/97
8/29/97
8/29/97
8/29/97
' 8/29/97
Time
1300
1300
1300
1300
1300
0900
0900
0900
0900
0900
Q900
0900
1500
1500
15.PO
1500
1500
1500
1530
153
153
153
0
0
F
1536
1530
1530
Field Sample ID
-M29-1-FHAR
-M29-1 -Filter
I-M29-1-HNO3
l-M29-1-KMnO4
I-M29-1-HCP
O-M29-FB-FHACE
O-M29-FB-FHAR
O-M29-FB-Filter
O-M29-FB-HNO3
O-M29-FB-BHAR
O-M29-FB-KMnO4
O-M29-FB-HCI
I-M29-2-FHACE
I-M29-2-FHAR
J-M29-2-Filter .
I-M29-2-HNO3
-M29-2-KMnO4
-M29-2-HCI
-M29-3-FHACE
-M29-3-FHAR
-M29-3-Filter
-M29-3-FH Catch
-M29-3-HNO3
-M29-3-HNO3
-M29-3-BHAR
Sample Description
FH0.1 NHNO3 Rinse
Beaker No. M-3
5% HNO3 / 10% H2O2 Absorbing Solution
10% H2SO4 / 4% KMnO4 Absorbing Sol.
8NHCI Rinse
FH Acetone Rinse - Beaker No. W-12
FH.0.1 N HN03 Rinse
Filter M97-0 17
5% HN03 / 10% H2O2 Absorbing Solution
BH0.1 NHN03 Rinse
10% H2SO4 / 4% KMnO4 Absorbing Sol.
8N HCI Rinse
FH Acetone Rinse - Beaker No. M-19
FH0.1 NHNO3 Rinse
Filter No. 97-016, 1002 - Beaker No. M-17
5% HNO3 / 10% H2O2 Absorbing Solution
10% H2SO4 / 4% KMnO4 Absorbing Sol.
8N HCI Solution
FH- Acetone Rinsa - Beaker No. M-21
FH0.1 NHN03 Rinse
Filter M97-0010 - Beaker No. M-20
Front Half Catch
5% HN03 / 10% H202 Absorbing Solution
5% HNO3 / 10% H2O2 Absorbing Solution
BH0.1 NHNO3 Rinse
Analysis Requested

MM
•
•
•


•
•
*
•
•


•
*
•
•


•
•
•
•
•
•
•
Hg
•
•
•
•
•
•
•
•
•
•
•
•
•
*
•
•
•
•
•
»
•
•
•
•
•














• «(

























































































i


























Remarks
•

Filters M010, 011, 012, 014, 015
Bottle 1/2




Petri Dish













Zip-lock Bag
Bottle 1/2
Bottle 2/2


-------
  O PACIFIC ENVIRONMENTAL SERVICES. INC.
                           , r.v_i. DUX
Research Triangle Park, North Carolina 27709-2077'
           (919) 941-0333 FAX: (919) 941-0234
                                                    Chain of Custody Record
Project Num
s4 13-004
Project Name fcfvr/fty 7=±&ujr „
US EPA EMC Asphalt Cement, '«fcA I .t
Samplers:
Oickerson, McDonald, Thompson, Dougherty, Hamilton
Date
8/29/97
8/29/97
•



Time
1530
1530




Field Sample ID
-M29-3-KMnO4
-M29-3-HCI

i


Relinquished by: (Signature)
A
Relinquished by: (Signature)
Ftetiqguishedytfy: (Sig/ature)
•qftuT--
, Date/Time
Date/Time
Date/Time

-------
II Custody Seal : Absent Sample Seals: Absent
|| Chain of Custody : Present Container. . . : Intact
|| Sample Tags : Absent
|| Sample Tag Numbers: Not Listed on Chain of Custody
I) SMO Forms : N/A
II 	 	
H Ice Chest/Box NO COOLANT
||TLI Number Client Sample ID 	 Matrix
||mR/H:CPM 	 Client COC ID 	 * Location 	
TLI Project Number 43411 Book ||
Client: PES03 - Pacific Environmental Services H
184
Date Received | 09/26/97 | ^/^/Tj^tWp/ Pa9B
Carrier and Number | HAND DELIVERED 84
To LAB To STORAGE
Date/Init Date/Init
|| 	 . 	 — ••
||l84-84-lA 0-M29-1-FHACE FH ACE RNS|
|| 0-M29-1-FHACE METALS LAB
II 	
||lB4-84-lB ' O-M29-1-FHAR FH0.1NHNO3
H 0-M29-1-FHAR METALS LAB
II 	 	
H184-84-1C 0-M29-1-FILTER FILTER)
I) 0TM29-1-FILTER METALS LAB
(184-84-10" 0-M29-1-HN03 : 5% HNQ3/10% H202 1
|| ' 0-M29-'»-HNQ3 *'' METALS LAB
||184-M-1E 0-M29-1-HNOJ $tyl J* HNOJ/10* H202
j| 0-M2J-l-lpJ*^fVt^ V*41^ HBTM>S, IAB
|| 	 	 • 	 ^ 	 — ».
H184-84-1F 0-M29-1-BHAR BM O.ltt HHO3 RNS
|| 0-M29-1-BHAR METALS LAB


|| 	 _ 	 	 	
1(184-84-10 0/M2S-1-KMN01 10* HI804/4VKMNO4 1
|| . 0-M29-1-KMN04 METALS LAB
|J- 	 — — " ' "; '
JJ184-84-1H 0-M29-1-HCL 8N HC1 1
|| 0-M29-1-HCL METALS LAB '
lil84-84-2A 0-M29-2-FHACE PH ACE RNSJ .
|| O-M29-2-FHACE METALS LAB
j|_ 	 . 	 	 	 • 	
||184-S4-2B 0-M29-2-FHAR ttt 0.1N HN03 1
|| O-M29-2-FHAR METALS LAB
|il84-84-2C 0-MJ9-2-FILTER FILTERJ
|| 0-M3f-3-FILTER METALS LAB
Jl 	 	 	 . ' " 	 - 1
JJ184-84-2D 0-M39-2-HN03 6lHN03/10*H2O2 1
|| . 0-M29-2-HN03 METALS LAB
||!84-84-2E O-M29-2-HN03 S*HN03/10%H202 1
|| ' OJ-M29-2-HN03 METALS, LAB
	 , 	 j - • 	 • 	 	 • 	
||l84-84-2F OJ-M29-2-BHAR BH 0.1HN03 RNS
|| Q/-M29-3-BKAR MBtALS LAB











To LAB
Date/Init






•:
'
-

,
-




To STORAGE
Date/Init
	












To LAB
Date/Init
	 1
	 )
	 	 	






1 	
i
| 	 j



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Date/Init


	






1 	 1
1 	 1

1 	 1

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Date/Init
i 	 1
i 	 1
i 	 1






i 	 1
i 	 1
i 	 1


To STORAGE
Date/Init
	 1
1 	 1
	





'


	 1
1 	 1


DISPOSED
Date/Init












1
1 	 B

(Deceiving Remarks:-'i 1-M29-2-BHAR was not on COC but was received. Sample 0-M29-FB-FILTER is marked 0-M29-2-FILTER but
j|_ ' ' has the date B/27/97 which l» the same as the COC.
jj ' Archive Remarks : '"-
=Form Revised 05/27/1997 -- Page 1 OF 4

-------
=TRIANGLE LABORATORIES,  INC.  -- LOG IN RECORD/CHAIN OF CUSTODY=
|| Custody Seal : Absent Sample Seals: Absent
II Chain of Custody : Present Container...: Intact
1) Sample Tags : Absent
|| Sample Tag Numbers: Not Listed on Chain of Custody
|| SMO Forms : N/A
TLI Project Number 43411 | Book
Client: PES03 - Pacific Environmental Services |
| 184
Date Received j 09/26/97 j By ^3 ^/Jlfl tAjLjl^/^ Pa9B
SI 1 / w — - i
H Ice Chest/Box NO COOLANT Carrier and Number | HAND DELIVERED | 84
IJTLI Number 	 Client Sample ID 	 Matrix
||mR/H:CPM. 	 Client COC ID. * Location. . .

1)184-84-20 0-M29-2-KMN04 10% H2S04/4 VKMN04
|| ( ' 0-M29-2-KMN04 METALS LAB
»'
H184-84-2H ' 0-M29-2-HCL 8N HCL
1) O-M29-2-HCL METALS LAB
||l84-84-3A 0-M29-3-FHACE FH ACE RNS
|| O-M29-3-FHACE METALS LAB
||184-B4-3B 0-M29-3-FHAR FH 0 . IN HN03
|j ' O-M29-3-FHAR METALS LAB
||l84-84-3C' 0-M29-3-FILTER FILTER
|| O-M29-3-FILTER METALS LAB
|)184-B4-3D 0-M29-3-HN03 5%HNQ3/10%H202
D 0-M29-3-HNO3 METALS LAB
»'
H184-84-3E OrM29-3-HN03 5%HNO3/10%H202
fl . O-M29-3-HN03 METALS LAB
D184-84-3F O-M29-3-BHAR BH 0.1N HN03
|| O-M29-3-BHAR METALS LAB '
1)184-84-30 O-M29-3-KMN04 10%H2SO4/4%KMN04
1) 0-M29-3-KMN04 METALS LAB
||l84-84-3H 0-M29-3-HCL 8N HC1
D O-M29-3-HCL METALS LAB
H '*
H184-B4-4A I-M29-1-FHACE FH ACE RMS
1) I-M29-1-FHACE METALS LAB
.
1)184-84-48 I-M29-1-FHAR FH 0.1N HN03
U . I-M29-1-FHAR METALS LAB
'
|)l84-84-4C I-M29-1-FILTER FILTER
II ' I-B29-1-FILTER METALS LAB j
II ) 1
I To LAB
Date/Init








•




II • j 1
||l84-84-4D IvM29-l-HN03 5%HN03/10*H202 1
[ I>M29-1-HN03 METALS LAB j
To STORAGE
Date/Init














I To LAB
Date/Init














To STORAGE
Date/Init














To LAB
Date/Init










1



To STORAGE
Date/Init

,












To LAB
Date/Init

-












To STORAGE
Date/Init














DISPOSED
Date/Init













1
|f"sjteceiving Remarks :•'! I-M29-2-BHAR was n>t on COC but was received. Sample 0-M29-FB-FILTER is marked 0-M29-2-FILTER but
|| 'has the date 8/27/97 which is the same as the COC.
II
H ' Archive Remarks:
          .Form Revised 05/27/1997  --  Page  2  OF 4*

-------
=TRIANGLE LABORATORIES,  INC. -- LOG IN RECORD/CHAIN OF CUSTODY*
jj Custody Seal : Absent Sample Seals: Absent
H Chain of Custody : Present Container...: Intact
|| Sample Tags : Absent
ij Sample Tag Numbers: Not Listed on Chain of Custody
I) SMO Forms , : N/A '
TLI Project Number 43411 Book ||
Client: PES03 - Pacific Environmental Services H
184 ||
ji /) II
1 1 J \n LLt~*~ "
Date Received | 09/26/97 | By^J^ /f, jM ./JTW^ Pa9"
II 	 	 	 — - . i / v -
|| Ice Chest/Box NO COOLANT Carrier and Number | HAND DELIVERED 84
||TLI Number Client Sample ID. . . . j 	 Matrix
||mR/H'CPM Client COC ID .... * Location 	

	 - "• " •
||l84-84-4E I-M29-1-KMN04 10*H2SO4/4%KMNO4
|| I-M29-1-KMN04 METALS LAB
	 " 	 	
||184-S4-4F I-M29-1-HCL 8N HCL
|| I-M29-1-HCL METALS LAB
||!84-84-5A O-M29-FB-FHACE FH ACE RNS
I) 0-M29-FB-FHACE METALS LAB
»•
||184-B4-5B 0-M29-F(B-FHAR "" , . JH0.1HNO3
H 0-M29-FB-FHAR >.'*' METALS*LAB
». ' ''" " ...-•.-
. ., , , i ...
||184-B4-5C 0-M29-2-FILTER 8/27/97 FILTER
|| 0-M29-FB-FILTER • METALS LAB
	 1 	 	 	 — 	 "' "'
||l84-84-SD 1 0-M29-FB-HN03 .. 5%HNQ3/10VH202
|| O-M2S-FP-HN03 | MEtALS LAB
	 	 	
||l84-84-5E OWm-FB-BHAH BH 0.1N HN03
y . • 0-M29-FB-BHAR MKtALS LAB
	 _ , . _ . . .
||184-B4-5F 0-M29-FB-KMN04 10»HJS04/4%KMNO4
|| 0-M29-FB-KMN04 MBTALS LAB '
	
|| 184 -84 -SO 0-M29-FB-HCL 8N HC1
|| 0-M29-FB-HCL HBtALS LAB
||!84-84-6A I-M29-2-FHACE rH ACE RNS
U I-M29-2-FHACE METALS LAB
||184-B4-6B I-M2I-2-FHAR FH 0 . 1HN03
g I-M2»-2-FHAR MEtALS LAB
	 	 • •--
||l84-84-SC I-M29-2-FILTER FILTER
H I -M29-2- FILTER MEtALS LAB
il84-84-6D I-M29-2-HN03 9*HN03/10%H202
IJM29-2-HN03 MEtALS LAB
i
Hf
| To LAB To STORAGE
Date/Init Date/Init








-




!
||l84-84-6E IvM29-J-KMN04 iO»H2S04/4%KMN04 1
|| liM29-2-KMN04 METALS LAB |










| To LAB
Date/Init














To STORAGE
Date/Init









	 1




To LAB
Date/Init





'



i*1
1 	 1
i
	


I
To STORAGE
Date/Init










	 	 1


i
To LAB
Date/Init
l





(



I 	 	
-


To STORAGE
Date/Init










	
	 _


DISPOSED
Date/Init














|| Receiving Remarks: -1 I-M29-2-BHAR was not oh COC but was received. Sample 0-M29-FB-FILTER i« marked C-M29-2-FILTER but
|| • ' 'h»« the date 8/27/91 which is the same as the COC.
u ;'
|| ' Archive Remarks:
          »Form Revised 05/27/1997  --  Page  3  OF  4*

-------
II Custody Seal : Absent Sample Seals: Absent
II Chain of Custody : Present Container...: Intact
|j Sample Tags : Absent
jj Sample Tag Numbers: Not Listed on' Chain of Custody'
|| SMO Forms : N/A
TLI Project Number 43411 Book
Client: PES03 - Pacific Environmental Services
184
Date Received | 09/26/97 | By ^J f\ Ji(> jfuT. — Pa9e
|| Ice Chest/Box NO COOLANT Carrier and Number HAND DELIVERED 84
||TLI Number 	 , Client Sample ID ' Matrix
||mR/H:CPM. ....Client COC ID * Locatipn
||
||184-B4-6F I-M29-2-HCL 8N HCL
jj ' I-M29-2-HCL i METALS LAB
||l84-84-6G I-M29-2-BHAR BH 0.1N HNO3
II (Not Listed-Client COC] * METALS LAB
J
SV i
||184-B4-7A I-M29-3-FHACE FH ACE RNS
II I.-M29-3-FHACE METALS LAB
1
||l84-84-7B I-M29-3-FHAR FH 0.1HN03
|| ' I-M29-3-FHAR METALS LAB
||l84-84-7C I-M29-3-FILTER FILTER
I) I-M29-3-FILTER METALS LAB
||184-S4-7D I-M29-3-FH CATCH FRONT HALF CATCH
|| I-M29-3-FH CATCH METALS LAB
II
||lB4-84-7E I-4W9-3-HNO3 5VHN03/10VH2O2
I) • 1 I-M29-3-HNO3 METALS LAB
• II
||!84-84-7F I-M29-3-HNO3 5%HNO3/10%H202
II I-M29-3-HNO3 METALS LAB
|
||184-B4-7G I-M29-3-BHAR BH 0.1N HN03
|| I-M29-3-BHAR METALS LAB
||184-B4-7H I-M29-3-KMN04 10% H2SO4/4* KMN04
|| I-M29-3-KMNO4 METALS LAB
II ' '*
B184-84-7I I-M29-3-HCL 8N HCL SOLN
H I-M29-3-HCL METALS LAB
||
II
II
|| . , , .
! 1
II v
IL >
| To LAB
Date/Init


'











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Date/Init














j To LAB
Date/Init














To STORAGE
Date/Init














j To LAB
Date/Init










1



To STORAGE
Date/Init














| To LAB
Date/Init

1












To STORAGE
Date/Init











"" " ' 	


DISPOSED
Date/Init




1
n









(LORecciving Remark* i •" I-M29-2-BKAR was not on COC but was received. Sample 0-M29-FB-FILTER is marked 0-M29-2-FILTER but fl
H ' )has the date 8/27/97 which is the same as the COC, II
I ' Archive RemarksJ
                                                                 •Form Revised 05/27/1997 -- Page 4 OF 4s

-------
oject
         43-4)1
                                                                                                        Anrjlyles  '
                                                                                            ICP  - GFAA   FI.AA  CVAA

jfe/lnt.: fef7 l())fijc)'7
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,
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                                     '  @
                                       IINO3
                                                                                                                       MCI
                                                              label
               VolunrieJiQ
         !eJfYrrcrss-
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                                                                                  i Volume
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                                                                                              (I DM Kg Spike loqulred)
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                                                                     .   ml lo	ml FV +..	uL Sc
                                                                     •             i
                                                                   InlllnU-

-------
                                                                                                l AA    TI.AA  CVAA
llent:
nte/lnt.:
                                       Triangle  Laboratories of RTP
                                                     (919)544-5729
lent Run//
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                                                    label
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                                                   •             \

                                                 Initials:	

-------
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                                                                                           ICP
                                                                                                  •  Ancjlyles  '
                                                                                               GPAA   R.AA  CVAA
ate/lnt.:_
                                       Triangle Laboratories of RTP   ,
                                                    (919)544-5729
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                                    lo 20 ml on
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                                                           label

                                                           Volume
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                                                                                                              ! ;abel %1'W
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                                                                                                 <   ml lo	ml FV +	uL Sc
                                                                                                              \

                                                                                                Inlllals:

-------
                                                                                                IUJ  • GPAA    TI.AA  CVAA
llenl:
nte/lnt.:
lent Run// lT-rf\c$' T"

Triangle Laboratories of RTP ,
(919)544-5729

i

	 1 	
               CONT II
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                                                     __j	ml lo	ml FV +	uL Sc
                                                     Inlllals:

-------
ojecl I,  43411
                                                                                                         Anrjlyles  '
                                                                                             ICP  • GFAA    PI.AA  CVAA
lent:
jte/lnt.:
Grit Runtf 0 -fll£$ - FBk
Trianale Laboratories of RTP .
(91 9> 544-5729
^ /"

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                                                                         »   ml to	ml FV -f	uL Sc

-------
                                                                                                 Gl AA   I:I.AA  CVAA
:llent:
•ate/lnr.:
                                       Triangle  Laboratories  of RTP
                                                     (919)544-5729
Merit Run//
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                     CONT //
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                                      Initials:	
                                           • ----- -                    4

                                      Hr-ilo*

-------
rojecl //.
                                                                                                 Anolyles  '
                                                                                      ICP - GPAA   IM.AA  CVAA
are/lnt.:
                                      Triangle Laboratories of RTP
                                                   (919)544-5729
Merit Run//
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                                                                                           FH & OH Serial dllullon performed

                                                                                           ,  •  ml lo	ml FV +	uL Sc

-------
                                                          PAGE  W'
                      INORGANICS SPIKE LOG
DATE
PROJECT *

SAMPLE IDs
ANALYTE
                                  ORIGINAL
                                  STANDARD
                                     #  -
ORIGINAL
STANDARD
 CONC.
 (PPM)
                                                   SPIKE
                                                   SAMPLE
 FINAL
VOLUME
 (ml)
 SPIKE
SAMPLE
 (PP8)
              INITIALS'
WITNESS-
                                                          •*"
                                                             -SF
               - LCS
                                                      ,926
                                               SE.
                  MSD
                         4-
                                                      (&?.
                                                             i
        /*?/ -fc -J/
                         Jr
                       3-68-3
                            *»
                       /OS/*.
              -M AS
       490501) - LdS
                       s-m-n
                            i
           m
      1
               -*•
          3-013-3
           ' ^ ~ I '3-*-

                                  3-
  qa\forms\inospke.log (08/22/96)
                                                                  57

-------
EXPdate

 2/1/98
 9/1/9«
 2/1/98
 9/1/98
 2/1/98
 2/1/98
 9/1/98
-9/1/98
 9/1/98
 9/1/98
 9/1/98
 9/1/98
 9/1/98
 9/1/98
 9/1/98
 -2/1/98
 9/1/98
 9/1/98
 8/1/98
 9/1/98
 9/1/98
 2/1/98
 8/1/98
 9/1/98
 9/1/98
 9/1/98
 9/1/98
 9/1/98
 9/1/98
 9/1/98
 9/1/98
 8/1/98
           SEE SPIKE LOG
Spiking Standard Preparation
Dement Standard Orig. Std. Spike(uL) cone
. 10
aJ»&»r#
ni^piM*
M
W
)
Ja/sS&ssS:
tfKtm
!a
!a
«d*'HB.ii'fii
:o '—-4
:r •. --
'M -J"W«*
'•9
'•»
<
<
*g
Ag
In -
do
Ja
via
* •%.- •,-

ib ~~s
>•

n '--•••*
i

rjf^-~
*a-iis-4v
3-oioW
2-115-4
3-010-7
2-115-4
2-115-4
3-010-10
3-010-10
3-012-7
3-010-10
3-010-10
3-010-10
3-010-10
3-012-6
2-115-4
3-012-5
3-010-10
3-010-8
3-010-10
3-010-10
2-115-4
3-010-9
3-010-10
3-010-10
3410-10
3410-10
3-010-10
3-010-10
3-010-10
3410-10
3-010-4
(ppm) Fvol(100mU (ppm)
wVX'M
-»'#
5000
950
5000
.
»--.»-r*?'

5
95
S
- *S'«S*.
- *s -^
s
95
'S&S ->•£
•i ,5 ,*
- -.s -••-
S
95
50
150
5
95
5
5
5
195
-•. 5
S r-
" S ^"
• -s .-
5
<-5 -.--
5
- S -«e-
15 V
SPIKING
rom Spiking Standard
pik*(uL) cone
FVd(100ml)
V^OOO ,**
•*HF«
1000
1000
1000
.«*tOOO-^s
-?*,iooo -"SSi
1000
1000
^.1000 ft?
1000 -
- 1000 A-
1000
1000
1000
1000
1000
1000
-1000 *
1000
1000
1000
-UC1000 --
1000 ?•
1000 T
1000 '
1000
4000 '
1000
--tooo ~
1000
(PPb)
•dM^"^
«»flL
50
950
so
#-50 *&
4i>ii'flO
so
950
ia»ao;vi
SOA«
.-.so
so
950
500
1500
SO

a SO
50
50
1950
--*»
so
so
•• so
•*>.
^90 -
50
*»M
S1SQ
combined
total
1000



1000




1000

2000

1000



2000







^ a»!
^200*%
"Spike separately
Bement   Orig Std    Spfl
-------
                                                               PAGE  1  OF 2
TRIANGLE LABORATORIES, INC.
Transfer Chain-of -Custody Form


Project
43411
Transfer From: IWLM To: IA I


Released by:
Initia-ls . .
flKJ'lL'
i "
Accepted by: VYI/A^"

MILES. ID
43411-
43411-
43411-
43411-
43411-
43411-
43411-
43411-
43411-
43411-
43411-
43411-
43411-
43411-
43411-
43411-
43411-
43411-
43411-
43411-
43411-
43411-
43411-
43411-
43411-
43411-
43411-
43411-
43411-
43411-


-000
-001
-002
-003
-004
-005
-006
-007
-008
-009
-010
-Oil
-012
-013
-014
-015
-016
-017
-018
-019
-020
-021
-022
-023
-024
-025
-026
-027
-028
-029

TLI No 	
TLI Blank
184-84-1A
184-84-1B
184-84-1C
184-84-1D
184-84-1E
184-84-1F
184-84-1G
184-84-1H
184-84-2A
184-84-2B
184-84-2C
184-84-2D
184-84-2E
184-84-2F
184-84-2G
184-84-2H
184-84-3A
184-84-3B
184-84-3C
184-84-3D
184-84-3E
184-84-3F
184-84-3G
184-84-3H
184-84-4A
184-84-4B
184-84-4C
184-84-4D
184-84-4E
Date 	 Time

_ts/_a/°n 2a-- ^

~ (.
Cust .Id 	
TLI Method Blank
O-M29-1-FHACE"
O-M29-1-FHAR
0-M29-1-FILTER
O-M29-1-HNO3
O-M29-1-HNO3
O-M29-1-BHAR
O-M29-1-KMNO4
O-M29-1-HCL
0-M29-2-FHACE
O-M29-2-FHAR
0-M29-2-FILTER
O-M29-2-HNO3
0-M29-2-HN03
0-M29-2-BHAR
0-M29-2-KMN04
O-M29-2-HCL
O-M29-3-FHACE
O-M29-3-FHAR
O-M29-3-FILTER
O-M29-3-HNO3
O-M29-3-HNO3
O-M29-3-BHAR
O-M29-3-KMNO4
O-M29-3-HCL
I-M29-1-FHACE
I-M29-1-FHAR
I-M29-1-FILTER
I-M29-1-HN03
I-M29-1-KMNO4
	 Y-F-v-r'OO I'Of^tr TT / r\i / n f \
iditional comments or  instructions:

-------
                                                                 PAGE 2  OF 2
                        TRIANGLE  LABORATORIES, INC.
                       Transfer Chain-of-Custody Form
                              Project  43411

                    Transfer  From:  IWLM     To:  IA I

                           IniZy&frs. .     Date. .., ._. A    Time . _. .

             Released by:
Accepted by: VYKA/V 1W l ( / ^~l et® •

MILES ID
43411-
43411-
43411-
43411-
43411-
43411-
43411-
43411-
43411-
43411-
43411-
43411-
43411-
43411-
43411-
43411-
43411-
43411-
43411-
43411-
43411-
43411-
43411-
43411-
43411-


-030
-031
-032
-033
-034
-035
-036
-037
-038
-039
-040
-041
-042
-043
-044
-045
-046
-047
-048
-049
-050
-051
-052
-053
-054

TLI No 	
184-84-4F
184-84-5A
184-84-5B-.
184-84-5C
184-84-5D
184-84-5E
184-84-5F
184-84-5G
184-84-6A
184-84.T6B
184-84'-6C
184-84-6D
184-84-6E
184-84-6F
184-84-6G
184-84-7A
184-84-: 7B
184-84-7C
184-84-7D
184-84-7E
184-84-7F
18.4-84-7G'.
184-84-7H
184-84-71
LCS , . . ,

Gust .Id 	
I-M29-1-HCL -
O-M29-FB-FHACE
0-M29-FB-FHAR
O-M29- 2 -FILTER 8/27/97
0-M29-FB-HN03
0-M29-FB-BHAR
0-M29-FB-KMN04
0-M29-FB-HCL
I-M29-2-FHACE
. I-M29-2-FHAR
I-M29 -2 -FILTER
I-M29-2-HN03
I-M29-2-KMN04 • , -
I-M29-2-HCL
I-M29-2-BHAR
I-M29-3-FHACE
I-M29-3-FHAR
I -M29-3 -FILTER
I-M29-3-FH CATCH
I-M29-3-HNO3
I-M29-3-HN03
I-M29-3-BHAR •/ ~ -•
I-M29-3-KMN04
I-M29-3-HCL
Lab Control Spike
Additional comments or instructions:
                                                      -XfrCOC  (Rev 11/01/94)-
                                                                     60

-------

-------
         * SEE SPIKE LOG
EXPtJat*

 2/1/98
 9/V98
 2/1/98
 9/1/98
 2/1/98
 2/1/98
 9/1/98
""9/1/98
 9/1/98
 9/1/98
 9/1/98
 9/1/98
 9/1/98
 9/1/98
 9/1/98
 2/1/98
 9/1/98
 9/1/98
 8/1/98
 9/1/98
 9/1/sa
 2/1/98
 a/i/sa
 9/1/98
 9/1/98
 9/1/98
 9/1/98
 9/1/98
 9/1/98
 9/1/98
 9/1/98
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3«m«nt

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Spiking Standard P
'Standard Orig. Std.
ID '"(ppm)
2-115-4
3410-10
2-115-4
3-01 0-7
2-115-4
2-115-1
34fO-10
3410-10
3412-7
3410-10
3410-10
•3410-10
.3410-10
3410-ld
341 2-8
2-115-4
3412-5

3410-fl
3410-10
3410-10

3410-9
3410-10
3410-10
3410-10
341O-10
3410-10
3410-10

3410-10
3410-6
100
100
100

100
100
100 -
100
10000
100-
100
100
100
100
10000
1000
10000
100
10000
100
100
100
10000
100
100
100
100
100
100
100
100
1000
reparation
Spike(u(J cone
Fvd(ICOmL) (ppm)
5000
5000
5000
950
5000
5000
5000
5000
950
5000
5000
5000
5000
5000 ~
950
5000
1500
5000
950
5000
5000
5000
1950
5000
5000
5000
5000
5000
5000
5000
5000
1500
5
5
5
95
5
5
5
5
95
S
5
5
5
5
95
50
150
5
95
5
5
5
195
5
5
5
5
5
5
5
5
15
SPIKING
rom S pitting Stand ml
SpikefrL) cone
=Vd(100ml)
1000 >
1000
1000
1000
1000
1000
1000
1000
1000
1000
1000
1000
1000
1000
1000
.-' 1000
1000
1000
tooo •
1000
1000
1000
1000 1
1000
1000
1000
1000
1000
tooo
1000
1000
1000
(ppb)
so
so
so
950
so
50
so
-so
950
so
so
so
50
SO '
950
SCO
1500
50
' 950
so
50
so
1SSO
so
50
so
50
so
so
so
so
ISO
combined
total
1000

1000
.*
1000
2000
1000

2000

20O'
1000UL ol the Spitang Standard gives tfie listed concl of «• «Oov» eicmtnu. ,
Element   Orig Std    Spik«(ul)     cone
           (ppm)   FvdQOOm    (ppbl
Au
C«
U
P
Pd
Pt
S
SI
Sn
S/
1000
1000
1000
1000
• 1000
1000
1000
10000
1000
1000
14O
30
70
100
160
300
350
350
20
5
1400
300
700
1000
1600
3000
3500
35000
200
SO
         Spiking Standard 3-013-3
         EXP: 11/26/97

         Spiked by:
         Pradigeatloev
         Postdigeatfon-  f
                                                                                                              :.r
                                                                                                                   ..:   62

-------
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-------
                                                                                                     PAGE 1 OF 5
 Project:  43411
                                      TRIANGLE LABORATORIES, INC.
                              Sample  Preparation Tracking & Management Form
                                                             Client: Pacific Environmental Services (PES03)
•^3
t/Acids() :  jf1
 Method
 Solvent/Acids
                   U
                                                Sample Information
                                Extraction Date:
                                  Lot:
      I   TLI        /
Sample] SAMPLE ID   /     CLIENT
#  crd]            /     SAMPLE ID
                             I         I      I
                             | Sample  (Final  |
                             |Wgt / ToN Volume |	/	/_
                             | g  / fcl J  ml  |
      | TLI Blank
000   |
                        Method Blank |
                                            L
                                        «*>
      | 184-84-1A
001
                             |
                 O-M29-1-FHACE |
                                                  I
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      | 184-84-1B
002
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                                            I
                                            1
      | 184-84-1C/V-B
                                 5   i  itoj
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004   |
                             i    5   IKS.!
                             i -^•••~« "i "i1    " '7*'
                             1    £>   '100   '
      1 184-84-1E
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                                            1
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                                            i \i\t~,  i
      | 184-84-2A
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                             I         I      I
                  0-M29-2-FHAR |
        184-84-2C/}$
 Oil
  Comments:
                                                                                           -REV 07/26/93  (PSTMF 7)--
                                                                                                     64

-------
                                                                                                       PAGE 2 OF  5
                                           TRIANGLE LABORATORIES, INC.
                                   Sample Preparation Tracking 6 Management Form
ject: 43411                                                          Client: Pacific Environmental  Services (PES03)
iod:
/ent/Acids() :
                                               Sample Information
mm
                              Extract ii
                                Lot:
                                Sample Infi
                        .Date: jifl/S]
                                                                      H3
  |   TLI         /                 | Sample   |Final |           |
-;.e|  SAMPLE ID    /    CLIENT       |Wgt / rfolV Volume |	/	/	|
rd|             /    SAMPLE ID     I 9  / t1/  ml  I           I
                                                                                                  '	I
  |  184-84-2E
                                              1
                     O-M29-3-FHACE  |
    184-84-3B
                      0-M29-3-FHAR
    184-84-3DE;
    184-84-3E
                      O-M29-3-HN03
            I
0-M29-3-HN03 |
                             I      i
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   | 184-84-3F
   | 184-84-3G
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                       5   '  ,-oo
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   | 184-84-3H
   | 184-84-4A                      |         |       I
   |                  I-M29-1-FHACE |         |       |
                                                         \oS-X
                                                                                             -REV 07/26/93 (PSTMF
                                                                                                      65

-------
          99
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-------
                                                                                                            PAGE 4 OF 5
                                              TRIANGLE LABORATORIES,  INC.
                                     Sample Preparation Tracking t Management Form
iject: 43411                                                             Client: Pacific Environmental Services  (PES03)
hod:
vent/Acids ( ) :
H
                                                  Sample Information
                                Extract!
                                  Lot:
   |   TLI
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          /
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            I         I       I
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'	/	I   Ifr*/	|	/	/	|	/	/	|	/	/	|	/	/	|
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                     1       1
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                                                               /    i
     184-84-7B
                                                    i
                        I-M29-3-FHAR
         .W:.1
-------
                                                                                                      PAGE 5 OF 5
 Project:  43411
                                             TRIANGLE LABORATORIES, INC.
                                     Sample Preparation Tracking t Management Form
                                                                    Client:  Pacific Environmental Services  (PES03)

 Solvent/Acids ():
                                 Extraction Date:
                                  Lot:
                                                Sample Information
      |   TLI         /
Sample| SAMPLE  ID    /    CLIENT
i  crd|            /    SAMPLE ID
                            III          I
                            | Sample*]Final  |          |      \^
                            | Wgt /Vofll Volume |	/	/	| _J&X$i
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                       0
                                 5   '   i»
   Comments:
                                                                                              -REV 07/26/93 (PSTMF 7).
                                                                                                       68

-------
                                                                                                             PAGE 1 OF 1
ject:  43411
                                              TRIANGLE LABORATORIES,  INC.
                                     Sample Preparation Tracking & Management  Form
                                                                        Client: Pacific Environmental Services
                                                                                                              (PES03)
lod:
/ent/Acids() :
                               Sample Information
              Extraction Date:,	/	/
                                                                i
                                                                                i
  |    TLI         /
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| Wgt  / fco\ | Volume |	/	/	|	/	/	|	/	/	|	/	/	|	/	/_
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TLI Method Blank |
          |
I

I
                                       5
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                                                 /   DPS
                                                                                                  	                  f
                                                                                                  -REV 07/26/93 (PSTMF 7)--*
                                                                                                             69

-------
                                                          PAGE
                         MERCURY SPIKE LOG
  DATE
PROJECT #

SAMPLE IDs
                        ORIGINAL
                         SPIKE
                        CONC. (Hg)
STANDARD #
 WORKING
 STANDARD
 P.REPARED
  FROM
 SPIKE
AMOUNT
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SAMPLE
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                                                          INITIALS
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                              \
   qa\forms\hgspke.log (08/22/96)
                                                                     70

-------

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Analvsis Report       Avenges          '    Hon  10-20-97 Ob:30r53 AM    page 19
Hftthnd: TRIAN6I.?   Sainl*  N«P:  1CSAR                   Operator:  OXH
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Analysis Report       Average*          •   Hon 10-20-97 06:30iS3  AH    page 23
Method:  TRIAHG12   Sasple tlaie: 184-84-1A8C POS         Operator:  OKH
Run TiiP:  10/20/97  03:43           Filename:  101^7
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                                      •   Mon 10-20-97  0^:30*53 AM    page 2?
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      is Report
.   Hon 10-20-97 06:30:>5 flH    page 43
Method:  TRl«Hfil.2   Saiple Ha»e:  ICV/CCV               Operatar:  OKH
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-------
Loc.  Concentration
  0
  1
  £
  4
  5
  &
  7
  8
  9
 10
 11
 12
 13
 14
 15
 1&
 17
 18
 19
 £0
 £1
 ££
 £3
 £4
 39
50.0 ug/L
100.0 ug/L
     ID/Weight File: EB17£.IDW

Solut ions

Calib.  Blank / Diluent / ICB / CCB
Stock        rbd'SP
Stock / Recovery Stock |->-&3-
ICV=30ug/L  U "    "
                      CHECK LO
                      43411 MB
                      43411 LCS
                      184-84-IftBC
                      184-84-lflBC L
                      184-84-£ftBC
                      184-84-3flBC
                      184-84-4ftBC
                      184-84-5ftBC
                      184-84-&ABC
                      184-84-7flBCT>
                      184-84-1DE
                      184-84-1DE L
                      184-84-£DE
                      184-84-3DE
                      184-84-4D
                      184-84-5BD
                      184~84-feD
                      184-84-7EF
                      Modifier 1
                                                              112

-------
Element File: TL.GEL
-Iement:  TI
^rint Data: Main+Suppl.
:'rint: Calib. Curve
                                    finalyst: HOLSTE
                                    Peak Storage: 1 Repl./Sample
INSTRUMENT: 4100 ZL
Wavelength: £76.8 Peak
Signal Type: Zeeman Aft
?ead Time: 5.0
Sample Replicates: S.
Standard Replicates: 2
                                    Technique: HGft            Version: 7.30
                                    Slit: C. 70 Low
                                    Signal  Measurement:  Peak  Area
                                    Read Delay:  0.0           BOC Time: 2

                                    Spike Replicates:  Same  as Sample
;ALIBRATION:
Solutions 1 ID
1
lalib. Blank 1 STD BLK
Standard 1 ISTDl=£5ug/L
Itandard £ ISTD£=50ug/L
Standard 3 1 STD3=100ug/L
ieslope Std. I50ug/L


Diluent Location: 0
Modifier #1 Location: 39
Calibration Units: ug/L
Calibration Type: Linear

Cone 1 Location
1
_ _«. _ _ 1 (7i

£5.01 1
50. 0 I 1
100.01 £
50. 0 I 1
I _



Volume

£0
10
£0
£0
£0
£0


Diluent M
Volume 4t
5
15
5
5
5
5


odi f i er
1 #£
5
5
5
5
5
5

Modifier #£ Location:
Sample Units: ug/L




urnace Time/Temperature Program:
tep Temp Ramp Hold IGas Flow Read Gas Type
1 110 5 3® 1 £50
£ 130 1 35 1 £50
3 700 5 £0 1 £50
4 1600 051 0
5 £500 1 5 1 £50
Norm
Norm
Norm
* Norm
Norm
njection Temp: £0 Pipette Speed: 85%















Extraction System: On
 EQUENCE:
 tep  Action  and  Parameters
  1    Pipet  diluent  •*•  modifier 1  + spike
  £    Run  HGA  steps  1  to  End
                                             sample/std
 HECKS:
 ecalibration  Type:
 ocations:  None
                     Reslope
 one.  Above  Calibration  Action:  Dilute
 Iternate  Sample Volumes (uL>:  5,£,1
 un  Alternate Volume Blanks:  Yes
                                        & Reanalyze After  1 Rep
  f  %RSD >  £0.0      and Concentration > 1.7      then Retry  1
  leek  %RSD on: Samples + Standards + Spikes + QC Samples
                                                                 t imes
  ecovery Measurements:
    uL  of 100 ug/L Standard at Location £  Gives     £5.0 ug/L
  ?asure  Recovery on Samples: 9,10,17,18
  id  to QC Samples: Yes               % Recovery Limits: 75 to 125
                                                                 113

-------
QC:
*H A/S I    QC Sample   I     Cone. Limits      I After(Periodic I At  I Count As I
  I Loc. I       ID       I   Lower     Upper     ICalibl  Check I End I Sample  I
1    4  ICV=30ug/L      £7.0       33.0
£    0  ICB             -£.0       £.0
3    5  CCV=fc0ug/L      48.0       7£. 0                 XX
4    0  CCB             -£.0       £.0                  XX
Run Periodic QC Samples:  Every 10
Out of Limit Actions Reslope and Rerun Samples

Matrix Check Calculations:
* Difference for Dupls: No     Locations:
% Recovery for Spike: No       Locations:         Cone:
                                                                114

-------
>ate:  10/31/97
)ata File: EB17£.DAT
'echnique: HGfl
  Tine:  05:41
  ID/Wt  File: EB17£.IDW
  Calib.  Type: Nonlinear
                      Slits 0.70  L
                      Lamp Current:
                      Energy: 49
     w A* A* A* A/ *V A* Af A* A/ Af A/ A* Af A* A/ A* A* A* A* A* A* A* A/ A/ A/ A* A/ A/ *V A/ A* A* A* A* A* A* A» Af A* A* A* «
      ID: STD  BLK
  Seq.  No. :  00001
          fl/S Pos. :  0
                                                                     Date:  10/31/97
iL  dispensed:  5 from 0, 5  from 39, £0  from 0
leplicate   1                              Time: 05:43
'eak  flrea  (ft-s):  -0.000                  Peak Height  (ft):  0.007
Background  Pk  flrea :  0.001         Background Pk Height   : 0. 1

 L  dispensed:  5 from 0, 5  from 39, £0  from 0
 eplicate   £  (Peak Stored)               Time: 05:46
 eak  flrea  (fl-s):  -0.001                  Peak Height  (fl):  0.007
 ackground  Pk  flrea (fl-s):  0.001         Background Pk Height  (fl):  0.008
 lank Corrected Pk flrea  (fl-s): -0.001
 oncentration  (ug/L  ): -0.5
 ean Cone   (ug/L  ) :

 uto-zero performed.
-0.£
SD: 0.38
                                       RSDC/.) :  175.09
 A, A, A, A, A, A, A, A, A, A, A/ A, A, A, A, A, A, A, A, A, A, A, A. A, A, A, A, A, A, A, A, A, A, A, A, A. A, A, A, A, A, A, A, A, A- A, A, A, A, A/ A, A, A, A, A, A, A, A. A/ A, A, A, A, A, A, A, A, A, A, A. A. <\. «V\. A* A, <\. •-
 1     ID: STDl=£5ug/L         Seq. No. : 0iZi00£    fl/S Pos. : 1      Date: 10/31/97

 L  dispensed: 15 from 0, 5 from 39, 10 from 1
 eplicate  1                             Time: 05:49
 eak flrea (fl-s): 0.035                  Peak Height  (fl): 0. 04&
 ackground Pk flrea (fl-s): 0.8££        Background Pk Height  (fl): 0.0£5
 lank Corrected Pk ftrea  (fl-s): 0.036
 oncentration  (ug/L  ): £3.1

 L  dispensed: 15 from 0, 5 from 39, 10 from 1
 eplicate  £  (Peak Stored)
 eak flrea  (fl-s):  0.034
 ackground Pk  flrea (fl-s):  0.0£1
 lank Corrected  Pk flrea  (A-s): 0.034
 oncentration  (ug/L  ):  ££.3
             Time:  05:5£
             Peak Height (fl): 0.043
             Background Pk Height  (fl): 0. 0£fe
 ean Cone   (ug/L  ):
££.7
 bandard number 1 applied.   C£5.03
 orrelation  coefficient:  1.00000
SD: 0.57
             Slope:  0.0014
                                       RSD(*) :  £.
 VA, A, A, A, A, A- A, A, A, A, A, A, A, A, A, A/ A, A, A, A, A, A, A, A, A, A, A, A, A, A, A, A, A, A, A, A, A, A, A, A, A, A, A, A, A, A, A, A, A, A, A, A, A, A, A, A, A, A, A, A, A, A, A, A, A, A, A, A, A, A, A. A, A, A, A, A,

 1     ID: STD£=50ug/L         Seq.  No. :  00003    fl/S Pos. : 1
                                        Date:  10/31/97
 _  dispensed:  5 from 0,  5  from 39, £0  from 1
 ?plicate   1                              Time: 05:55
 sak flrea  (fl-s):  0.077                   Peak Height  (fl): 0.087
 nckground  Pk  flrea (fl-s):  0.041         Background Pk  Height  (fl):  0.053
 Lank Corrected Pk flrea  (fl-s): 0.078
 jncentration  (ug/L  ):  55. fe
                                                                   115

-------
Peak Area  :  0.076
Background Pk Area  (A-s>:  0.043
Blank Corrected Pk  Area :  0.077
Concentration  (ug/L  ): 54.8
                                 Peak Height  (A):  0.088
                                 Background Pk  Height (A): 0.048
Mean Cone   : 1.11
                    A* A# A/ A/ A* A* A/ A* A/ *
Tl
ID: STD3=100ug/L
Seq.  No.: 00004
                                                 ft/S Pos.:  £
Date: 10/31/9
uL  dispensed:  5 from 0,  5 from 39, £0 from 2
Replicate   1                            Time: 06:01
Peak  Area  :  0.150                 P»ak Height  (A):  0.165
Background Pk  Area (A-s): 0.086        Background Pk  Height  : 0.098
Blank Corrected Pk Area  (A-s): 0.151
Concentration   
-------
L dispensed:  15  from  0,  5 from 39,  10 from 1
eplicate   1                            Time: 0&:0S
'eak Area   : 0.024
lank Corrected Pk  Area :  0.018        Background Pk Height  (ft): 0.023
lank Corrected Pk  Area 
-------
Calihratinn -
                            118

-------
ates 10/31/97                Time:  06:19                    Slit: 0.70  L
ata File: EB 172. DOT         ID/Wt  File: EB17S. IDW          La»p Current:  0
echnique: HGA                Calib.  Type: Linear            Energy: 5S

V A* A/ A/ *U A* A* A/ A/ A* A* A/ A/ A/ A* A* A* A* A/ A/ A/ A/ A/ A/ A/ A/ A* A* A* A* A* A* A/ A* A* A/ A* A/ A* A* A* A/ A/ A/ A* A/ A/ A/ A* A/ A* A/ A/ A/ A* A* A/ A/A/A/ A/A*A*A* A/A/Ar A/A/A*A*A/A« A« A*A**W*
1    ID: ICV=30ug/L         Seq. No. :  00006    A/S Pos. :  4     Date:  10/31/97

_ dispensed: 5 from 0,  5 from 39,  £0 from 4
splicate  1                             Time: 06:22
eak Area  (A-s) :  0. 04£                  Peak Height  (ft): 0.049
ackground Pk flrea 
-------
Background Pk Area (A-s):  0.084         Background  Pk Height  A#A*^*A* AfAsAr As A«A«A/ArAf ArA*A/A*Ar A*A« A? A* A**
Tl     ID: 43411  MB            Seq. No.:  00009     A/S Pos. : 7      Date:  10/3i/«

uL dispensed: 5  from 0,  5  from 39, £0  from 7
Replicate  1                              Time: 06:40
Peak Area (A-s>: -0.001                  Peak Height (ft):  0.007
Background Pk ftrea   : -8.884                  Peak Height (ft):  8.887
Background Pk  Area  (A-s):  8.884    ,     Background  Pk Height  (A): 8.807
Blank  Corrected  Pk Area  (A-s): -8.004
Concentration  (ug/L  ):  -2.4

Mean Cone   (ug/L  ):        -1.3         SD: 1.58                  RSDC/.):  113.3

A/ A/ A/ A/ A/ A/A/ A* A* A/ A/ A* A/ A* A* A/ A/ A* A* A/ A* A* A* A/ A* A* A* *V A/ Af A* A* A* A* A*A*Af *V A* A* A* AvA»A» A»A# A* A* A* A* A* A* A* »VA*A»A**WA* A/A*A»A*A* A* A*A»*WA» A* A*Av*\* A* A/A*
Tl     ID: 43411  LCS           Seq. No. : 80010     A/S Po*.s  8      Date: 10/31/

uL dispensed:  5  from 8,  5  from 39, £0  fro« 8,
Replicate   1                              Ti«*: 06:45
Peak  Area  (A-s): 0.847                   Peak Height  (A)s  8.051
Background Pk  Area  (A-s):  8.838         Background Pk Height  : 0.034
Blank  Corrected  Pk  Area  (A-s): 8.848                     '
Concentration  (ug/L   ) :  3£. 1
 uL dispensed: 5 from  8,  5 from  39,  20 fro»  8
 Replicate   £ (Peak  Stored)              Times «6i48             U>-3-*7 «
 Peak Area  (A-s): 8.854                  Peak Height  (A)s  0.062
 Background  Pk Area  (A-s): 8.833        Background Pk  Height  

 uL dispensed: 5 from  8,  5 from  39,  20 from  9          „
 n_f^r^_rL->yivi|^ivji^j^,i^,j^,j\ri^jv>^(\,i\jn-ronj'\jn_ir\j HJ HJ HJ |}j'lVii*^i'^n»r>jwv^'^•^•^••^•^<^»^«^»t^>^^»^"y^*%«jVT»'^j'^'\»"W~wf^^"^T^^-^r^f
 Tl    ID:  43411 LCS           Seq.  No.s 00012    A/S Pos.: 8      Datei 10/31,

 uL dispensed: 5 from  0,  5 from  39,  20 from  8
 Replicate   1                             Time: 06:52
 Peak Area  (A-s):  8.855                  Peak Height  (A) s 0.864
 Background Pk Area (A-s): 8.831        Background Pk  Height  (A):  0.037
 Blank Corrected Pk Area  (A-s):  0.056
 Concentration  (ug/L   ):  37.4
                                                                         120

-------
>ak  Area : 0.052                   Peak Height   :  0.060
ickground Pk Area   : 0.053
mcentration  :        36.4         SD: 1.50                 RSDC/):  4.14

t Ay Av Ay Av Av Ay Ay Ay A* Ay Ay Av Av Ay Ay A* Av A* Av Av A* A* Ay Ay Ay A* A> Ay Ay Ay Av Ay Ay Ay Ay A* Ay Ay A* Ay A* A* Ay Ay Ay Ay Ay Ay Ay Av Ay Ay A/Ay Ay Ay Ay Ay AyAy Ay Ay AyAy AyAy AyAyAy AyAy Ay Av Ay AyA* •"W
     ID: 184-84-lflBC        Seq. No. : 00013    ft/S Pos. : 9     Date:  10/31/97

. dispensed: 5 from  0,  5 from 39,  £0 from 9
 plicate  1                             Time: 06:58
 ak  flrea (ft-s): 0.001                   Peak Height  :  0.007
.ckground Pk Area  3     Seq.  No.: 00014    A/S  Pos.: 9     Date:  10/31/97
 . dispensed:  5  from 39,  5 from  £,  £0 from 9
 plicate   1                             Time: 07:04
 ak Area  (A-s):  0.031                  Peak Height  (A):  0.050
 ckground  Pk  Area (A-s): 0.018         Background Pk  Height  (A): 0.035
 ank Corrected  Pk Area  (A-s): 0.031
 ncentration  (ug/L  ): £1.1

 . dispensed:  5  from 39,  5 from  £,  £0 from 9
 plicate   £  (Peak Stored)              Time: 07:07
 ak Area  (A-s):  0. 0£9                  Peak Height  (A):  0.051
 .ckground  Pk  Area (A-s): 0.019         Background Pk  Height  (A): 0.034
 ank Corrected  Pk Area  (A-s): 0. 0£9
 ncentration  (ug/L  ):  19.7

 an Cone   (ug/L  ):       £0.4         SD: 0.96                  RSDC/O: 4.70

 covery is
                                                           ,^^^

     ID:  184-84-1ABC L       Seq.  No. : 00015     A/S Pos. : 10     Date:  10/31/97

  dispensed:  5 from 0,  5 from  39,  £0 from 10
 plicate   1                             Time: 07:10
 ak Area  (A-s):  -0. 00£                 Peak Height (A): 0.005
 ckground  Pk  Area (A-s): 0.003        Background  Pk Height  (A):  0.007
 ank Corrected Pk Area  (A-s):  -0.001
 ncentration  (ug/L  ): -0.9
                                                                   121

-------
Peak flrea (ft-s): -0.001                  Peak Height  (ft):  0.007
Background Pk ftrea  (ft-s):  0. 00£         Background Pk Height  (ft): 0.008
Blank  Corrected Pk ftrea  (ft-s) :  0.000
Concentration (ug/L   ):  0.0

Mean Cone  ^^ A»A»^^^*^^A» Ar^to *VW A*
Tl      ID: 184-84-2flBC          Seq.  No. :..00flU7    ft/S Pos. s  11    Date:  iC/31/

uL  dispensed:  5 from  0,  5 from 39,  £0 from 11          ::
Replicate   1                             Time: 07:££
Peak  ftrea  (fl-s): 0.002                  Peak Height  (ft):  0.007
Background  Pk ftrea (fl-s): 0.000         Background Pk Height  (ft) s  0.007
Blank  Corrected Pk flrea  (fl-s): 0.003
Concentration (ug/L  ):   1.9

 uL  dispensed:  5 from 0,  5 from 39,  20 from  11
 Replicate   £  (Peak Stored)              Time: 07:24
Peak flrea  (fl-s):  -0. 00£       .          Peak Height  (ft):  0.007
 Background  Pk flrea (fl-s): 0.000   .  ',-.• Background Pk Height  (ft) :  0. 007
Blank  Corrected Pk flrea  (fl-s): -0.001
 Concentration (ug/L  ):  —0.8

 Mean Cone  (ug/L   ):        0.6         SD*  1.96                  RSD<*>  s 347.fi

 r^i\tf^*\fr^i^f\fi\^i\ff^i\t*\t'\f'^r^t\f*\f*\ti\tt\f'\ft\t*^
 Tl      ID:  184-84-3flBC       ^Sfc.Q.  No. s 00018     ft/S Pos. :  1£     Date:  10/31/

 uL dispensed: 5 from 0,  5 from 39, £0  from  12
 Replicate  1                              Time:  07:£7
 Peak  flrea (fl-s):  -0.003         ,         Peak Height   (ft):  0.008
 Background  Pk flrea (fl-s):  0.005         Background Pk Height  (ft):  0.009
 Blank  Corrected Pk flrea  (ft-s):  -0.002
 Concentration  (ug/L  ):  -1.4
                                                                      122

-------
eak ftrea  (ft-s): -0.001                  Peak Height  (ft): 0.009
ackground  Pk ftrea  (ft-s):  0.003         Background Pk Height   : 0.009
lank Corrected Pk ftrea  (ft-s):  -0.001
oncentration (ug/L   ):  -0. A

ean Cone   :  77.18

1     ID:  184-84-4ftBC         Seq. No. :  00019    ft/S Pos. :  13    Date:  10/31/97

L dispensed: 5 from 0,  5 from 39, £0  from 13
ample  abs.  is greater  than that of  the largest standard.
eplicate   1                             Time: 07:33
eak firea  (ft-s): 0.162                   Peak Height   A/ A/ *VW A* *V A* A* A* A* A^ A* *\* A/ A* A* *V^^ A/ A/ A* A/ A/ A/ A/ A/ A* A* A/ A^ A^ A* A* A^ A^ A* A^ A^ A^ A* ''v A* A* A* A/ •"
1     ID:  184-84-4ABC 2.A     Seq. No. :  00020    fi/S Pos. :  13    Date:  10/31/97
 - dispensed: 20  from  0,  5 from 39,  5  from 13
 eplicate  1                             Time: 07:36
 eak  Area (A-s):  0.091                   Peak Height  (A):  0.265
 ackground Pk Area  (A-s): fl. 355         Background Pk  Height (A): 0.209
 lank Corrected Pk  Area 
-------
e\f A/ A* A/ A* A/ A* A* A* A* A* A* A* A* A/ A/ A* A* A* A* A» A* Af Af A* A* A* A» A* A* A* A* A* A/ A» A* A* A* A* A* A* A* A/ *V A* A> A* A/ A* A* Ar A* A» A* A/ Ar ArAs A*A**V Ar A*A* A*A* A* Ar A* A* A* A* A* Ar A/ A*Ai
Tl    ID: CCB                 Seq. No. : 00022     A/S Pos. : 0      Date: l®/31/ : 0.005
Blank Corrected Pk  Area A#*V^A» A*
Tl     ID: 184-84-5ABC        Seq.  No. s 00023    A/S Pos.:  14    Date:  10/31/

uL dispensed: 5 from 0, 5 from 39,  20 from  14
Replicate  1                             Time: 07:53
Peak Area (A-s): -0.001                 Peak Height (A): 8.007
Background Pk Area  (ft-s) : -0. 002        Background Pk Height  ^»n*A» A* A*A* A# A* A* A*A»A*A* A*A» A*A* A> A* A* A* A^Af A* A/A* A/ A* A* A*Ay A» A» A» A* AA*
 Tl    ID: 184-84-6ABC         Seq.  No.:  00024    A/S Pos.: 15    Date:  18/31/

 uL dispensed: 5 from 0, 5 from 39, 20  from 15
 Replicate   1                             Time: 07:59
 Peak Area  (A-s): 0.125                  Peak Height   :  0.263
 Background  Pk Area  (A-s): 0.587         Background Pk  Height'  : fc,257
 Blank Corrected Pk Area (A-s): 0.-126
 Concentration (ug/L   ): 84.3

 uL dispensed: 5 from  0, 5 from 39, 20  from 15
 Replicate   2  (Peak Stored)              Tine: 08:02
 Peak Area  (A-s): 0.129                  Peak Height  (A) s  0.289
 Background  Pk Area  (A-s): 0.546         Background Pk  Height 
-------
AtAtAtArAtAtArArA* ArAtAtAtAtAtArAtAtAtAtAtA* AtAtArArAt AtArArAtAtAtArAtAtAtAr AsArArArArArArAtArArAr ArArAtA**
ID: ia4-84-7flBCbc«,
                             Seq. No
                                        000£5
                                                 ft/S Pos. : 16
                                                                  Date:  10/31/97
L dispensed:  5  from 8,  5 from 39,  £0  from 16
eplicate   1
eak ftrea  (ft-s):  0. 03£
ackground  Pk  ftrea  :  0. 0£9
ackground Pk  ftrea (ft-s) : 0.581
lank Corrected  Pk ftrea : 7.63
                                                                   125

-------
                                        *V *\* *\* »\e A* A* A*
Tl
      ID: 184-84-1DE L
                             Seq.  No.:  00028
fl/S Pos. :  18
Date: 18/31/c
uL dispensed: 5 from 0, 5  from  39,  £0
Replicate   1
Peak ftrea  (fl-s) : 0.000
Background  Pk flrea  (fi-s) :  -0.001
Blank Corrected Pk  Area  
 Tl
       ID:  184-84-£DE
                              Seq.  No.:  00030
                                                  fl/S Pos.:  19
                                                                   Date:  10/31
 uL dispensed:  5  from  0,  5 from 39,  £0 from 19
 Replicate   1                            Ti«e: 08:34
 Peak flrea  (fl-s):  0.001                  Peak Height  
-------
i\t f\f f\f *v A* A* At At At At At At At A* At A/ At Af A* Af Af At At At At At At At At At At At At At A» At A* At At A» At At Af At At At At At At At At At At At At At At At At At At At At At Ar At AtAr At Af At AtAr A*
1    ID:  184-84-3DE          Seq. No. : 00031    A/S Pos. : 20    Date: 10/31/97

L dispensed: 5 from 0, 5 from 39, £0 from £0
eplicate   1                            Time: 08:40
eak Area  (A-s) : 0.001                  Peak Height  (ft): 0.007
ackground  Pk Area  (A-s): 0.001        Background Pk Height  : 0.011
lank Corrected Pk Area  
-------
   At At A/ At At At At At At At At At A/ At At At At At At At A* At At At At A* At At At A/ A* At At At At At At A* At At At A* At At At At At At At A* At At At At At At At At At At At At At At A* A* At A* At**
   Tl    ID:  CCB                Seq.  No.: 00034    A/S Pos. : 0     Date:

   uL dispensed: 5 from 0, 5 from 39,  £0 from 0
   Replicate   1                            Tin*: 08:58
   Peak Area  (A-s): -C. 801                 Peak Height (ft): 0.007
   Background Pk Area  (A-s) : -0.000        Background  Pk Height  (A): 0.00
   Blank Corrected Pk Area (A-s): 0.000
   Concentration (ug/L  ): 0.1

   uL dispensed: 5 from 0, 5 from 39,  £0 from 0
   Replicate   2. (Peak Stored)              Time: 09:01
   Peak Area  (A-s): -0.001                 Peak Height (A): 0.007
   Background Pk Area  (A-s): 0.001         Background  Pk Height  (A): 0. 0e
   Blank Corrected Pk Area (A-s): 0.000
   Concentration (ug/L  ) : 0. 1

I  Mean Cone    (ug/L  ):        0.1         SD: 0. 06                  RSD(*)

   QC  sample  is within range —2.0  —  S. 0
   *V -^t*vAtA/Af *v Af At *\r At At At At *V *V At A/ *V A/ *V *V *\t A» A/ A* A*A»A»AyA^Ar^>*V*VA» Ay Af A»Ar At At At At At At At At A/ At A> A»At AtAt At AtAt AtAt At At AtA»*W At A»A**
   Tl     ID: 184-S4-5BD          S«q.  No. : 00035    A/S Pos. : 22     Date

   uL  dispensed: 5 from 0, 5 from 39, £0 from  £2
   Replicate  1                            Time: 09:04
   Peak  Area (A-s): 0.001                  Peak Height (ft): 0.006
   Background Pk Area  (A-s): -0.001       Background Pk Height  (A) s 0.0
   Blank Corrected Pk Area  (A-s) s 0.002
   Concentration  (ug/L   ):  1.5     '

   uL  dispensed: 5 from 0, 5 from 39, 20 from  £2
   Replicate  £  (Peak Stored)              Time: 09:107
   Peak  Area (A-s): -0.001                 Peak Height (A): 0.007
   Background Pk Area  (A-s): 0.001        Background Pk Height  (A) s 0.  :  0.008
    Background  Pk  Area (A-s): -O. WMB        Background Pk Height (A) s 0. »
    Blank Corrected Pk Area  (A-s) : 0.002
    Concentration  (ug/L  ):  l.£

    uL dispensed:  5 from 0,  5 from 39, 20  from £3
    Replicate   2  (Peak Stored)              Time: 09il3
    Peak Area  (A-s):  -0.003                 Peak Height  (A):  0.009
    Background  Pk  Area (A-s> : -0.000        Background Pk Height XA) s 0.
    Blank Corrected Pk Area  (A-s): -0.002
    Concentration  (ug/L  ):  -1.5
                                                                        i:

-------
k* A^ *W A* A* A* A* A* A* A* A/ *V ^^ A* A^ A* A* A* ^^^w A* A/^^ A* A/ A/ A**V A* A* A»*W*^ A* A* A/ A/ A*
L     ID: 184-84-7EF          Seq.  No. : 08837     A/S Pos. :  £4    Date:  10/31/97

. dispensed: 5 from 0,  5  from 39,  £8 from £4
?plicate  1                            Time: 89:16
»ak Area (A-s): -8.881                 Peak Height  (A> :  8.888
jckground Pk Area  (A-s):  -8.881       Background Pk Height (ft): 8.886
:ank  Corrected Pk Area  (A-s): -8.881
mcentration (ug/L  ):  -8.4

. dispensed: 5 from 8,  5  from 39,  £8 from £4
splicate  £  (Peak Stored)             Time: 89:19
>ak Area (A-s): -8.888                 Peak Height  (A):  8.888
\ckground Pk Area  (A-s):  -8. 88£       Background Pk Height (A): 8.885
ank  Corrected Pk Area  (A-s): 8.881
mcentration (ug/L  ):  8.4

•an Cone  (ug/L  ):         8.8        SD : 8.53                 RSDC/O:  £878.85
                                     A*A/A*A/A/A*A*A^

     ID: CCV=68ug/L          Seq.  No. : 88838     A/S Po's. :  5     Date:  18/31/97

.  dispensed: 5 from  8,  5 from 39,  £8 from  5
 plicate  1                            Time: 89 : ££
 ak Area (A-s): 8.888                  Peak Height (A): 8.145
.ckground Pk Area  (A-s): 8.849        Background  Pk Height (A): 8.891
 ank Corrected Pk  Area  (A-s): 8.881
ncentration (ug/L  ):  54.5

  dispensed: 5 from  8,  5 from 39,  £8 from  5
 plicate  £  (Peak  Stored)              Time: 89:£5
 ak Area (A-s): 8.891                  Peak Height (A): 8.148
ckground Pk Area  (A-s): 8.855        Background  Pk Height (A): 8.894
 ank Corrected Pk  Area  (A-s): 8. 89£
ncentration (ug/L  ):  61.6

 an Cone   (ug/L   ):        58.8        SD :  5.81                 RSD(%):  8.64

:  sample is within range 48.8 - 7£. 8
     ID: CCB                 Seq. No. : 88839     A/S Pos. : 8     Date:  10/31/97

  dispensed: 5  from  8,  5 from 39, £8 from  8
 plicate  1                            Time:  89:£8
 ak Area (A-s):  8.888                 Peak Height (A): 8.806
 ckground Pk Area  (A-s): -8. 88£       Background Pk Height  (A): 8.885
 ank Corrected  Pk  Area (A-s): 8.881
 ncentration  (ug/L  ): 8.7

  dispensed: 5  from  8,  5 from 39, £8 from  8
 plicate  £  (Peak  Stored)              Time:  89:31
 ak Area (A-s):  -8. 88£                Peak Height (A): 8.885
 ckground Pk Area  (A-s): 8.883        Background Pk Height  (A): 8.888
 ank Corrected  Pk  Area (A-s): -8.881
 ncentration  (ug/L  ): -8.9
                                                                    129

-------
QC sample  is within range -£. 0 - 2. ©
                                                              130

-------
Height  File: AB826.IOH
pie Volume: 100 il
                              t:  D.STREETER-EOHARDS
                        Nonnal Weight:  1.0 g
oc.
Saiple  ID
                          Height
                                Dilution
ST BLANK
ST01:0.2ug/L
ST02=0.5ug/L
STD3=1.0ug/L
STD4:2.0ug/l
STD5:5.0ug/L
ST06:10.0ug/L
ICV:4.0ug/L
ICB
CHECK LO
43411 MB1
43411 MB1  D
43411 LCS1
43411 LCS1D
184-84-ICA8
184-84-1CAB D
184-84-1DE
184-84-1DE D
184-84-10E MS
184-84-1DE MSD
CCVl=6.0ug/L
CCB1
184-84-1F
184-84-1F  0
184-84-16
184-84-16  D
184-84-1H
184-84-1H  0
184-84-2CAB
184-84-2CAB D
184-84-2F
184-84-2F  D
CCV2=6.0ug/L
CCB2
184-84-20E
184-84-2DE D
184-34-2DE MS
184-84-2DE MSD
184-84-26
184-84-26  D
184-84-2H
184-84-2H  D
184-84-3CA8
184-84-3CAB D
CCV3:6.0ug/L
CCB3
184-84-3DE
184-84-3DE D
184-84-3F
184-84-3F  D
184-84-36
184-84-36  D
184-84-3H
184-84-3H  D
                     —^  3-osu-?    ftSe   10
                                                                                            131

-------
Loc.
Saiple ID
Height
Dilution
54
55
56
57
58
59
60
61
62
63
64
65
66
67
68
69
70
71
72
73
74
75
76
77
78
79
184-84-4CA8
184-84-4CAB D
CCV4:6.0ug/L — ^ 3-022-tf
CCB4
184-84-4D
184-84-40 D
184-84-40 HS
184-84-4D HSD
184-84-4E
184-84-4E D
184-84-4F
184-84-4F D
184-84-5CAB
184-84-5CAB 0
CCV5:6.0ug/L 	 ^3-033l-£ N
CCB5 '
184-84-580 "X
184-84-5BO 0
184-84-5E V v.l \^
184-84-5E 0 /• U^'
184-S4-5F I p-'f^
184-84-5F D L PC^l*
184-54-5GF OUUL/TO vV
184-84-56F D
CCV6:6.0ug/L j
CCB6
                                            \o
                                                                                 132

-------
tent File: H6..MEL
lent: Hg2
it Data: Main+Suppl.
it: Calib. Curve
 rks:
.NDARDS: 3-023-3
 3-022-8
 RUMENT: 5100
 length: 253.7 Peak
 al  Type: AA
  Tine: 30.0
 le  Replicates: 1
 dard  Replicates: 1
Analyst:  0  STREETER-EDHAROS
Peak Storage: None
Technique:  MHS           Version: 7.01
Slit:  0.7  Low
Signal Measurement: Peak Height (5)
Read Delay:  1.0          80C Tine: 2
E:
e Type:
ant Flow
BRATION:
utions


K Bl 3nL>
U . o lanK
dard 1
dard 2
dard 3
dard 4
dard 5
dard 6
ibration
ibration
Air
: 10.0 L/min

: 10
i
!
t CTfi Dl K
( Of U DLft
ISTD i
iSTD 2
ISTD 3
ISTD 4
ISTD 5
ISTD 6
Units: ug/l
Type: Linear
Flame Sensor
Fuel Flow: 2

Cone |
t
t
	 i

0.200;
0.500|
}.000|
2.0001
5.000,'
10.000;
Saaple Units

: On
.0 L/ain












: ug/l

 ix Check  Calculations:
 fference  for Dupls: No     Locations:
 covery for  Spike: No       Locations:
              Cone:
                                                                                                           133

-------
Element File:  H6..HEL        Eleient:  Hg2
Date: 10/20/97               TIM:  12:48
Data File: AB826.DAT         ID/Ht  File: AB826.IDH
Technique: HHS               Calib.  Type:  Linear
fieiark 1: STAHDARDS= 3-023-3
Reaark 2: QC= 3-022-8
                             Wavelength:  253.?
                             Slit:  0.7 L
                             Laip Current:  0
                             Energy:  71
Hg2   ID: ST BLANK
Seq. Ho.:  00001    A/S Pos.: --    Date: 10/20/97
Replicate  1                           Tiie:  12:4°
Peak Area (A-s): 0.007                 Peak Height  (A): -0.000
Blank Corrected Pk Height (A): -0.000
Concentration (ug/L  ): -0.002

Auto-zero perforied.
Hg2   ID: STDl=0.2ug/L
Seq.  No.:  00002    A/S Pos.: -    Date: 10/20/9^
Replicate  1                           Tine:  12:53
Peak Area (A-s): 0.329                 Peak Height  (A): 0.014
Blank Corrected Pk Height (A): 0.014
Concentration (ug/L  ): 0.228

Standard number 1 applied.  [0.200]
Correlation coefficient: 1.00000       Slope:  0.0712
 Hg2    ID: STD2:0.5ug/L       Seq. No.: 00003    A/S Pos.:  -    Date:  10/20/9'

 Sample  abs.  is greater  than  that of the largest standard.
 Replicate   1                           Tine: 12:54
 Peak  Area (A-s):  0.794                 Peak Height (A):  0.034
 Blank Corrected  Pk  Height  (A):  0.034
 Concentration  (ug/L  ):  0.476

 Standard nunber  2 applied.   [0.500]
 Correlation coefficient:  0.99904       Slope: 0.0683
 Hg2   ID:  ST03=l.Oug/L       Seq.  No.:  00004    A/S Pos.: -    Date: 10/20/97

 Saiiple abs. is greater than that of the largest standard.
 Replicate  1                           Ti"e:  12:5S  ,
 Peak Area (A-s): 1.584                 Peak Height  (ft):  0.068
 Blank Corrected Pk Height (A): 0.068
 Concentration (ug/L   ): 0.991

 Standard  nuaber 3 applied.   [1.000]
 Correlation  coefficient:  0.99984       Slope: 0.0679
  Hg2   ID:  STD4:2.0ug/L       Seq.  No.:  00005    A/S Pos.: --    Date: 10/20/97

  Saiple abs.  is greater than that of  the largest standard.
  Replicate  1                           Tiie:  12:57
  Peak Area (A-s): 3.128                 Peak Height  (A): 0.136
                                                                                                                  134

-------
e.ntration (ug/L   ):  2.009

dard number 4  applied.   [2.000]
elation coefficient: 0.99997
          Slope:  0.0681
  ID: STD5=5.0ug/L
Seq. No.:  00006    A/S  Pos.: -    Date: 10/20/97
le abs. is greater than that of  the  largest standard.
icate  1                          Tiie:  12:58
 Area (A-s): 7.826                Peak  Height  (A): 0.341
k Corrected Pk Height (A):  0.341
entration (ug/L  ): 5.009

dard number 5 applied.  [5.000]
elation coefficient: 1.00000      Slope:  0.06S2
   10: STD6:10.0ug/L      Seq. No.:  00007    A/S  Pos.: --    Date: 10/20/9'

 le abs.  is greater than that of the largest standard.
 icate   1                           Time: 12:59
  Area  (A-s):  15.110                Peak Height  (A):  0.633
 k Corrected  Pk Height (A): 0.633
 entration  (ug/L   ): 9.282

 dard number  6 applied.  [10.000]
 elation coefficient: 0.99907       Slope: 0.0645
                                                                                                             135

-------
tieient me: HG..nEL      Eleient: Hg2
Date: 10/20/97           Tiie: 13:00
Data File: AB826.DAT       ID/Ht File: A8826.IDH
Technique: MHS           Calib. Type: Linear
Reiark 1: STANDARDS: 3-023-3
Reiark 2: QC= 3-022-8
                            Havelength: 253.7
                            Slit: 0.7 L
                            Laip Current: 0
                            Energy: 71
          H
Display  Calibration - C;\fflJJSER\MJ ILES\ELEHEHT\H6_.HEL
          0.633,
                                                   Linear
                                                   Com. Cocf.:  B.999B7
                                                   Slope:  8.8645	
                                        Concentration
                                                             1B.BB8
                                                                                 136

-------
nent File: H6..HEL        Eleient:  Hg2
:e: 10/20/97               Tile:  13:03
:a  File:  A8826.DAT         ID/Ht  File: AB826.IDW
Unique:  NHS               Calib.  Type:  Linear
lark  1:  STANDARDS: 3-023-3
:ark  2:  QC= 3-022-8
                                                      Wavelength: 253.7
                                                      Slit: 0.7 L
                                                      Laip Current: 0
                                                      Energy: 71
    ID:  ICV:4.0ug/L
                         Seq.  Ho.: 00008    A/S Pos.: --    Date: 10/20/97
 licate   1                           Tiie:  13:06
 k  Area  (A-s):  6.250                 Peak Height (A):  0.266
 nk Corrected  Pk  Height (A): 0.266
'centration (ug/L  ): 4.123
    ID:  IC8
                         Seq.  No.:  00009     A/S  Pos.:  --    Date: 10/20/97
 licate  1                           Tine: 13:08
 <  Area (A-s):  0.023                 Peak Height (A): 0.001
 ik Corrected Pk  Height  (A): 0.001
 :entration (ug/L  ):  0.017
                          Seq. No.: 00010    A/S Pos.: --    Date:  10/20/9"
   ID: CHECK LO

,icate   1
; Area (A-s): 0.338
ik  Corrected Pk Height (A): 0.014
:entration  (ug/L   ): 0.224
                                    Tine: 13:09
                                    Peak Height (A); 0.014
    ID:  43411 M81
                         Seq. No.: 00011    A/S Pos.:  -    Date:  10/20/9"
  icate  1                           Tine: 13:12
   Area (A-s): 0.006                 Peak Height (A): 0.000
  k Corrected Pk Height (ft):  0.000
  entration (ug/L  ):  0.006
    ID: 43411 M81 D
                         Seq. Ho.: 00012    A/S Pos.: --    Date:  10/20/97
  icate  1
   Area (A-s): 0.011
  k Corrected Pk Height (A):  0.000
  entration (ug/L  ): 0.006
                                   Time: 13:13
                                   Peak Height (A): 0.000
    ID: 43411 LCS1
                          Seq. No.: 00013    A/S Pos.: --    Date: 10/20/97
                                   Tine: 13:14
                                   Peak Height (A): 0.
  icate  1
   Area (A-s): 4.411
  ( Corrected Pk Height (A): 0.185
  jntration (ug/L   ): 2.868
    ID: 43411 LCS1D
                             .  No.: 00014    A/S Pos.: --    Date: 10/20/97
                                                                                                             137

-------
Peak Area (A-s):  0.149
Blank CorrectedPkej
                                           Height (A):  0.009
                      :  0.140
Hg2   ID: 43411 LCS1
                            Seq. No.: 00015    A/S Pos.:  --     Date:  10/20/97
Replicate  1                          Tiie: 13:22
Peak Area (A-s): 7.518                Peak Height (A): 0.323
Blank Corrected Pk Height (A):  0.323
Concentration (ug/L  ):  5.006
Hg2   ID:
 Replicate   1                           Time:  13:34
 Peak  Area  (A-s): 8.571                 Peak  Height  (A):  0.359
 Blank Corrected  Pk Height (A): 0.359
 Concentration  (ug/L   ): 5.563
 Hg2    ID:  43411  LCS1D
                             Seq.  No.:  00019    A/S Pos.: -    Date: 10/20/9'
 Replicate   1                           Time:  13:44
 Peak  Area  (A-s):  7.427                 Peak Height (A):  0.316
 Blank Corrected  Pk  Height  (A): 0.316
 Concentration  (ug/L  ):  4.900
                  ftfcC
Hg2   ID: 43411 LCS1D
Replicate  1
Peak Area (A-s): o'.274
Blank Corrected Pk Height (A):  0.014
Concentration (ug/L  ): 0.215
                                      Tine: 13:23
                                      Peak Heigh
Date: 10/20/9"
Hg2   ID: 43411 LCS1D
                             Seq.  No.:  00017
Replicate  1
Peak Area (AX:  0.166
                                       Tine:  13:30
                                       Peak Height  (A): 0.008
Blank Cprfected Pk Height (A): 0.008
Concsfitration (ug/L  ): 0.120
                              ec. No.:  00018     A/S  Pos.:  --
Oats:. 10/20/9
                             Seq. No.: 00020    A/S  Pos,:  --  .  Date:  10/20/9r
 Hg2    ID:  184-84-
 Replicate  1                           Tise: 13:45
 Peak Area (A-s):  0.026                 Peak HeighrM: '0.001
 Blank Corrected Pk  Height  (A): 0.001
 Concentration (ug/L  ):  0.022
 Hg2   ID: 184-84-ltAfrD      Seq. No.: 00021    A/S Pos.: -    Date: 10/20/9?

 Replicate  1                          Tiie: 13:46
 Peak Area (A-s):  0.011                Peak Height (A): 0.000
 Blank Corrected Pk Height (A):  0.000
                                                                                                                138

-------
I    ID:  184-84-1DE
Seq. No.:  00022    A/S Pos.: --    Date: 10/20/97
Jlicate   1                           Tine:  13:47
ik Area  (A-s):  0.027                 Peak Height (A):  0.001
ink Corrected  Pk  Height  (ft): 0.001
tcentration  (ug/L  ):  0.016
    ID:  184-84-1DE  D
Seq. No.:  00023     A/S  Pos.:  --     Date:  10/20/97
 licate  1                           Tiie: 13:48
 k Area (A-s):  0.022                 Peak Height (A): 0.001
 nk Corrected Pk Height  (A):  0.001
 centration (ug/L  ):  0.020
    ID:  184-84-1DE MS       Seq. No.: 00024    A/S Pos.: --    Date: 10/20/97

 licate   1                          Tine: 13:50
 k Area  (A-s):  4.055                Peak Height (A): 0.163
 nk Corrected Pk Height  (A):  0.163
 centration (ug/L  ):  2.521
    ID: 184-84-1DE USD     Seq.  No.: 00025    A/S Pos.: -    Date: 10/20/9'

 licate  1                          Time: 13:51
 k Area (A-s): 3.961                Peak Height (A): 0.163
 nk Corrected Pk Height (A):  0.163
 :entration (ug/L  ):  2.532
 licate  1
 < Area (A-s): 0.114
 ik Corrected Pk Hei
    ID: CCVU6.0ug/L
 Seq. No.: 00027    A/S Pos.: -    Date: 10/20/97
  .icate  1                           Time:  13:53
  ; Area (A-s): 8.003                 Peak Height  (A): 0.336
  tk Corrected Pk Height (A): 0.336
  :entration (ug/L  ): 5.216
    ID: CC81

  icate  1
   Area (A-s): 0.019
  k Corrected Pk Height (A): 0.001
  entration (ug/L  ): 0.016
 Seq. No.: 00028    A/S Pos.: --    Date: 10/20/97
          Tiie: 13:55
          Peak Height (A): 0.001
                                                                                                                139

-------
Hg2   ID:  184-84-1F

Replicate   1
Peak Area  (A-s):  0.025
Blank Corrected Pk Height (A): 0.001
Concentration (ug/L  ): 0.019
Seq. No.:  00029    A/S Pos.: -    Date:  10/20/97
          Tiie:  13:56
          Peak Height  (A): 0.001
Hg2   ID: 184-8MF D        Seq. No.:  00030    A/S Pos.: --    Date: 10/20/97

Replicate  1                           Ti»e: 13:57
Peak Area (A-s): 0.021                 Peak Height (A): 0.001
Blank Corrected Pk Height (A): 0.001
Concentration (ug/L  ): 0.012


Hg2   ID: 184-84-1G          Seq.-No.:  00031    A/S Pos.: --    Date: 10/20/97

Replicate  1                           Tine: 13:58
Peak Area (A-s): 0.112                 Peak Height (A): 0.005
Blank Corrected Pk Height (A): 0.005
Concentration (ug/L  ): 0.070


Hg2   ID: 184-84-1G D        Seq. No.:  00032    A/S Pos.: --    Date: 10/20/97

Replicate  1                           Time: 13:59
Peak Area (A-s): 0.115                 Peak Height (A): 0.005
Blank Corrected Pk Height (fl): 0.005
Concentration (ug/L  ): 0.072


Hg2   ID: 184-84-1H          Seq. No.:  00033    A/S Pos.: --    Date: 10/20/97

Replicate  1                           Tine: 14:00
Peak Area (A-s): 0.016                 Peak Height  (A): 0.001
Blank Corrected Pk Height (A): 0.001
Concentration (ug/L   ): 0.011


Hg2   ID: 184-84-1H  D        Seq. No.:  00034    A/S Pos.: --    Date: 10/20/97

Replicate  1                           Tine: 14:01
Peak Area (A-s): 0.005                 Peak Height  (A): 0.000
Blank Corrected Pk Height  (A): 0.000
Concentration (ug/L   ): 0.002

                                                      "   ~"          ---!-.-.-.-.--
Hg2   ID: 184-84-2SA6-        Seq. No.: 00035    A/S Pos,: --    Date: 10/20/97
                        ^  iv*-iite
Replicate   I                           Tiie: 14:02
Peak Area (A-s):  -0.000                Peak Height (ft):  Q.QOO
Blank Corrected Pk Height  (A): 0.000
Concentration  (ug/L   ):  0.006

                   f fee. <«r .0-3141««
Hg2   10: 184-84-2SA6  D       Seq. No.: 00036    A/S Pos.:  --    Date:  10/20/97
                                                                                                                    140

-------
^ Hiea
              -u.uvi
                                        neiyiu  \nj. -v.uuv
nk' Corrected Pk Height  (A):  -0.000
centration (ug/L  ):  -0.002
   ID: 184-84-2F
                        Seq. No.: 00037    A/S Pos.: --    Date:  10/20/97
licate  1                           Tiie:  14:04
k Area (A-s): -0.001                Peak Height  (A): 0.000
nk Corrected Pk Height (A):  0.000
:entration (ug/L  ): 0.000
   ID: 184-84-2F D

licate  1
< Area (A-s): 0.000
ik Corrected Pk Height (A):  0.000
rentration (ug/L  ): 0.000
                        Seq. No.: 00038    A/S Pos.: --    Date:  10/20/97
                                  Tiie: 14:06
                                  Peak Height (A): 0.000
   ID: CCV2:6.0ug/L
                         Seq.  No.:
A/S Pos.:  --     Date:  10/20/97
 iicate  1
 ( Area (A-s):
 ik Corrjfrt^Pk Height (A): 0.017
    rttion (ug/L  ): 0.263
                                  Time: 14:06
                                  Peak Height (A): 0.017
   ID:
                         Seq.  No.: 00040    A/S Pos.: -    Date: 10/20/9'
 .icate  1                           Time:  14:08
 ; Area (A-s): 8.437                 Peak Height  (A):  0.354
 ik Corrected Pk Height (ft): 0.354
 :entration  (ug/L  ): 5.493
   ID: 444
                         Seq.  No.:  00041    A/S Pos.: --    Date: 10/20/97
 .icate   1          " '               Time:  14:10
 ; Area  (A-s): 0.014                 Peak Height (A):  0.001
 ik Corrected  Pk Height (A): 0.001
 :entration  (ug/L   ): 0.012
   ID:  184-84-2DE

  icate   1
  Area  (A-s): 0.030
 ik Corrected  Pk Height (A): 0.001
  entration  (ug/L   ): 0.019
                         Seq.  No.:  00042    A/S Pos.: -    Date: 10/20/9'
                                   Time:  14:14
                                   Peak Height  (A): 0.001
                          Seq. No.: 00043    A/S Pos.:  --     Date:  10/20/97
  ID: 184-84-2DE D

icate  1
 Area (A-s): 0.031
k Corrected Pk Height (A):  0.001
                                    Tine:  14:15
                                    Peak Height (A):  0.001
                                                                                                         141

-------
Hg2   ID: 184-84-2DE HS      Seq.  No.:  00044     A/S Pos.:  -     Date:  10/20/97

Replicate  1                           Tiie:  14:16
Peak Area (A-s): 4.500                 Peak Height (A):  0.189
Blank Corrected Pk Height (A): 0.189
Concentration (ug/L  ): 2.922
^M****^****!********'**^!*******************^****^**^*^'************'*****'*'*'***'**'*****'**

Hg2   ID: 184-84-2DE HSD     Seq.  No.:  00045     A/S Pos.:  --     Date:  10/20/97

Replicate  1                           Tiie:  14:17
Peak Area (A-s): 4.192                 Peak Height (A):  0.175
Blank Corrected Pk Height (A): 0.175
Concentration (ug/L  ): 2.720


Hg2   ID: 184-84-26          Seq.  No.:  00046     A/S Pos.:  --    Date:  10/20/97

Replicate  1                           Tine:  14:17
Peak Area (A-s): 0.033                 Peak  Height (A):  0.002
Blank Corrected Pk Height (A): 0.002
Concentration (ug/L   ): 0.033


Hg2   ID: 184-84-2G  D         Seq. No.:  00047     A/S Pos.: -    Date:  10/20/97

Replicate  1                           Time:  14:18
Peak Area  (A-s): 0.145                 Peak Height (A): 0.006
Blank Corrected  Pk  Height  (ft): 0.006
Concentration  (ug/L   ):  0.093
 «**•>***« *
-------
icate  1                          Tiie: 14:22
 Area (A-s):  0.008                 Peak Height (A): 0.001
k Corrected Pk Height  (A): 0.001
entration (ug/L  ):  0.008
  ID: CCV3:6.0ug/L       Seq. No.: 00052    A/S Pos.: -    Date: 10/20/97

icate  1                          Tiie: 14:23
 Area (A-s): 9.918                Peak Height (A): 0.411
k Corrected Pk Height (A):  0.411
entration (ug/L  ):  6.372


  ID: CCB3               Seq. No.: 00053    A/S Pos.: --    Date: 10/20/97

icate  1                          Tine: 14:24
 Area (A-s): 0.040                Peak Height (A): 0.002
k Corrected Pk Height (A):  0.002  •   .
sntration (ug/L  ):  0.026


  ID: 184-84-3DE         Seq. No.: 00054    A/S Pos.: -    Date: 10/20/97

icate  1                          Time: 14:25
 Area (A-s): 0.035                Peak Height (A): 0.002
< Corrected Pk Height (A):  0.002
;ntration (ug/L  ):  0.025


  ID: 184-84-3DE D       Seq. No.: 00055    A/S Pos.: --    Date: 10/20/97

icate  1                          Tine: 14:26
 Area (A-s): 0.027                Peak Height  (A): O.OOi
< Corrected Pk Height (A):  0.001
;ntration (ug/L  ):  0.014


  ID: 184-84-3F          Seq.  No.: 00056    A/S Pos.:  -    Date: 10/20/97

icate  I                          Tine: 14:27
 Area (A-s): 0.008                Peak Height  (A): 0.001
< Corrected Pk Height (A):  0.001
 sntration (ug/L  ): 0.012


  ID: 184-84-3F D        Seq.  No.: 00057    A/S  Pos.:  --    Date: 10/20/97

 .cate   1                          Tine:  14:29
 Area (A-s): 0.008                Peak Height  (A): 0.000
 ; Corrected Pk Height (A):  0.000
 intration (ug/L  ): 0.006
  ID: 184-84-36
Seq.  No.:  00058    A/S Pos.:  --    Date:  10/20/97
                                                                                                            143

-------
oionn vuiiobtcu ri\ nciynu  \n i,  v.vv/
Concentration (ug/L  ):  0.107
Hg2   ID: 184-84-36 0        Seq.  No.:  00059    A/S Pos.: --    Date: 10/20/97

Replicate  1                           Tiie: 14:31
Peak Area (A-s): 0.157                 Peak Height (A): 0.007
Blank Corrected Pk Height (A):  0.007
Concentration (ug/L  ): 0.106


Hg2   ID: 184-84-3H          Seq.  No.:  00060    A/S Pos.: --    Date: 10/20/97

Replicate  1                           Tiie: 14:32
Peak Area (A-s): 0.026                 Peak Height (A): 0.001
Blank Corrected Pk Height (A):  0.001
Concentration (ug/L  ): 0.016


Hg2   ID: 184-84-3H D        Seq.  No.:  00061    A/S Pos.: --    Date: 10/20/97

Replicate  1                           Time: 14:33        . ••  •
Peak Area (A-s): 0.026                 Peak Height (A): 0.001
Blank Corrected Pk Height (A):  0.001
Concentration (ug/L  ): 0.019


Hg2   ID: ^^^CA^^^Se^.  No.:  00062    A/S Pos.: --    Date: 10/20/97

Replicate  1                           Tine:  14:34
Peak Area (A-s): 0.101                 Peak  Height (A):  0.004
Blank Corrected Pk Height (A):  0.004
Concentration  (ug/L   ): 0.059

                              iw:
Hg2   ID: 184-84-4CAfrD      Seq.  No.:  00063     A/S Pos.: --    Date: 10/20/97

Replicate   1                           Tine:  14:35
Peak Area (A-s):  0.096                Peak  Height  (A):  0.004
Blank Corrected Pk Height (A): 0.004
Concentration  (ug/L   ):  0.062


Hg2   ID: CCV4=6.0ug/L      Seq. No.: 00064    A/S Pos.: --  .  Datfi: 10/20/9'

Replicate   1                           Tine:  14:37
Peak Area (A-s):  8.394                Peak Height  (A):  0.359
Blank Corrected Pk Height  (A): 0.359
Concentration  (ug/L   ):  5.558
 Hg2   ID:  CCB4
Seq.  No.:  00065     A/S P
-------
2 .  ID:  184-84-4D

plicate  1
ak Area (A-s): 0.045
ank Corrected Pk Height (A): 0.002
ncentration (ug/L  ): 0.026
Seq. No.:  00066    A/S  Pos.:  -    Date: 10/20/97
          Tiie:  14:39
          Peak Height (A):  0.002
2   ID: 184-84-40 D    •    Seq. Ho.:  00067    A/S  Pos.:  --    Date:  10/20/97

plicate  1                           Ti»e: 14:40
ak Area (A-s): 0.030                 Peak Height (A):  0.001
ank Corrected Pk Height (A): 0.001
ncentration (ug/L  ): 0.016


I   ID: 184-84-4D MS       Seq/ No.:  00068    A/S  Pos.:  -    Date:  10/20/97

jlicate  1                           Tine: 14:41
ik Area (A-s): 4.079                 Peak Height (A):  0.168
ank Corrected Pk Height (A): 0.168
 icentration (ug/L  ):  2.599


 I    ID: 184-84-4D USD      Seq. No.: 00069    A/S Pos.:  --     Date:  10/20/97

 Jlicate   1                           Time: 14:42
 Jk  Area  (A-s):  4.112                 Peak Height (A):  0.170
 ink  Corrected Pk Height  (A): 0.170
 icentration  (ug/L   ):  2.631


 1    ID: 184-84-4E          Seq. No.: 00070    A/S Pos.:  -     Date:  10/20/97

  licate   1                           Tine: 14:43
 k Area (A-s): 0.096                 Peak Height (A):  0.004
  nk Corrected Pk Height (A): 0.004
 centration (ug/L  ):  0.061


    ID: 184-84-4E D        Seq. No.: 00071    A/S Pos.:  -     Date:  10/20/97

  licate  1                           Time: 14:44
 k Area (A-s): 0.073                 Peak Height (A):  0.003
  nk Corrected Pk Height (A): 0.003
  centration  (ug/L  ):  0.048
     ID:  184-84-4F

  licate   1
  (  Area  (A-s):  0.010
  ik Corrected  Pk Height  (A): 0.001
  :entration  (ug/L   ):  0.011
 Seq.  No.:  00072    A/S Pos.: --    Date: 10/20/97
           Tine:  14:45
           Peak Height (A): 0.001
                                                                                                               145

-------
Peak 'Area (A-s):  0.006                 Peak Height (A):  0.001
Blank Corrected Pk Height  (A):  0.001
Concentration (ug/L  ):  0.012
                     -
Hg2   ID: 184-84-5CW ^...^Se^.  Ho.: 00074    A/S Pos.: -•    Date:  10/20/97

Replicate  1                          Tiie: 14:47
Peak Area (A-s): 0.004                 Peak Height (A): 0.000
Blank Corrected Pk Height (A):  0.000
Concentration (ug/L  ):  0.005
,«.«,.^^...,.««...,^^.^^.

Hg2   ID: 184-84-5CA6 D       Seq.  No.: 00075    A/S Pos.: -    Date:  10/20/97

Replicate  1                          Tine: 14:49
Peak Area (A-s): 0.001            "     Peak Height (A): 0.000
Blank Corrected Pk Height (A):  0.000
Concentration (ug/L  ):  0.002


Hg2   ID: CCV5:6.0ug/L       Seq.  No.: 00076    A/S Pos.: --    Date:  10/20/97

Replicate  1                          Time: 14:50
Peak Area (A-s): 8.459                Peak Height (A): 0.354
Blank Corrected Pk Height (A):  0.354
Concentration (ug/L  ):  5.495


Hg2   ID: CCB5               Seq.  No.:  00077    A/S Pos.: --    Date:  10/20/97

Replicate   1                           Tine:  14:51
Peak Area (A-s):  0.029                 Peak Height (A):  0.001
Blank Corrected Pk Height (A): 0.001
Concentration  (ug/L  ):  0.017


Hg2   ID: 184-84-5BD        Seq. No.: 00078    A/S  Pos.: --    Date: 10/20/97

Replicate   1                           Time:  14:52
Peak Area (A-s):  0.014                 Peak Height  (A):  O.OOi
Blank Corrected Pk Height  (A): 0.001
Concentration  (ug/L   ):  0.012


Hg2    ID:  184-84-5BD D       Seq. No.: 00079    A/S  Pos.: -   Date: 10/20/97

 Replicate   1                           Tiie: 14:53
 Peak  Area  (A-s):  0.006                 Peak Heighf{A):  0.00.
 Blank  Corrected Pk Height (A): 0.001
 Concentration (ug/L   ):  0.009


 Hg2   ID:  184-84-5E           Seq. No.: 00080    A/S Pos.:  -    Date: 10/20/97
 Replicate  1
Tiie: 14:55
n..t. It*. £ _L A / A
                                                                                                               146

-------
I    ID:  184-84-5E D        Seq. No.: 00081    A/S Pos.:  -     Date:  10/20/97

)licate   1                           Tiae: 14:56
ik  Area  (A-s):  -0.003                Peak Height (A): -0.000
ink Corrected  Pk Height (A): -0.000
icentration (ug/L   ): -0.002


!    ID:  184-84-5F          Seq. No.: 00082    A/S Pos.:  --     Date:  10/20/97

>licate   1                           Tine: 14:57
•.k  Area  (A-s):  -0.001                Peak Height (A): -0.000
ink Corrected  Pk Height (A): -0.000
 centration (ug/L   ): -0.003


    ID:  184-84-5F  D       Seq. No.: 00083    A/S Pos.:  -     Date:  10/20/97

•licate   1                           Tine: 14:58
 k  Area  (A-s):  0.000                Peak Height (A): 0.001
 nk Corrected  Pk  Height  (A): 0.001
 centration (ug/L   ):  0.008


    ID:  184-84-5GF        Seq. No.: 00084    A/S Pos.:  --    Date:  10/20/9*

 licate   1                           Tine: 14:59
 k  Area  (A-s): 0.036                Peak Height (A): 0.002
 nk Corrected Pk  Height  (A): 0.002
 centration (ug/L   ):  0.026


    ID:  184-84-5GF D       Seq. No.: 00085    A/S Pos.: --    Date:  10/20/9"

 licate  1                          Time: 15:00
 k  Area (A-s): 0.015                Peak Height (A): 0.001
 nk Corrected Pk Height (ft):  0.001
 centration (ug/L  ):  0.008


    ID:  CCV6:6.0ug/L       Seq. No.: 00086    A/S Pos.: --    Date: 10/20/9"

 licate  1                          Tine:  15:01
 k Area (A-s): 6.713                 Peak Height  (A): 0.284
 nk Corrected  Pk Height (ft):  0.284
 centration (ug/L   ): 4.407


    ID: CCV6:6.0ug/L       Seq.  No.:  00087    A/S Pos.: -    Date: 10/20/97

 licate  1                           Tine:  15:06
 k Area (A-s): 5.871                 Peak Height  (A): 0.254
 nk Corrected  Pk Height (A):  0.254
  :entration  (ug/L   ):  3.932
147

-------
Replicate  1                          Tiie: 15:17
Peak Area (A-s): 5.836                Peak Height  (A): 0.263
Blank Corrected Pk Height (A):  0.263
Concentration (ug/L  ): 4.073
Hg2   ID: CCB6               Seq.  No.: 00089    A/S  Pos.: -    Date: 10/20/97

Replicate  1                         Tiie: 15:19
Peak Area (A-s):  -0.006               Peak Height (A):  -0.000
Blank Corrected Pk  Height (A): -0.000
Concentration (ug/L  ): -0.002
                                                                                                                148

-------
(eight File: A8827.IDH           Analyst: O.STREETER-EOHARDS
>le Volune: 100 iL               Noninal Weight: 1.0 g

>c.       Saaple ID       "  Weight       Dilution

 0     ST 81K
 1     8101:0.2119/1^
 2     STD2:0.5ug/L
 3     STD3--1.0ug/L   \^
 4     5TD4:2.0ug/L   f
 5     STD5:5.0ug/l   I
 6     5T06:lO.Oug/L  1
 7     ICV:4.0ug/l  IL__ 1  625-b    KG
 8     .IC8
 9     CHECK LO
 0     43411 M82
 1     43411 M820
 2     43411 LCS2.
 3     43411 LCS2D
 4     184-84-6CA8
 5     184-84-6CAB D
 6     184-34-60
 7     184-84-60 D
 8     184-34-60 MS            ,-•;'. ••' ;  ',
 9     184-84-60 USD
 0     CCV7:6.0ug/L   	 3-033-C*
 1     CCB
 2     134-S4-6G
 3     184-34-6G D
 4     1S4-34-5E
 5     184-34-6E D
 5     184-34-oF
 7     184-84-6F D
 3     1S4-34-7CDA8
 9     184-84-7COAB D
 )     184-34-7G
 1     134-84-7G D
 I     CCVS:6.0ug/L  	
 i     CCB
 <     1S-1-84-7EF
 5     184-84-7EF D
 5     184-84-7EF MS
 1     1S4-84-7EF MSD
 3     184-34-7H
 »     184-84-7H D
 )     184-34-71
 I     184-84-71 D
 I     CCV9:6.0ug/L    —
 i     43377 MSI
 t     43377 M81 D
 i     43377 LCS1
 .     43377 LCS10
      184-50-1CAB
 !     184-50-1CA8 0
      184-50-10
      184-50-10 D
      184-50-10 MS
      184-50-10 MSO
      CCVl:6.0ug/L   —
                                                                                                         149

-------
Loc.     Saiple ID       Weight  .   Dilution
54
55
56
57
58
59
60
61
62
63
64
65
66
67
68
69
70
71
72
73
74
75
76
77
73
79
SO
81
32
83
84
85
86
87
88
89
90
91
92
93
94
95
96
97
93
99
100
101
102
103
104
105
106
107
108
109
CCS ' -
184-50-1E
184-50-1E 0
184-50-1F
184-50-1F 0
184-50-16
184-50-1G 0
184-50-2CA8
184-50-2CA8 0
184-50-20E
184-50-20E 0
CCV2=6.0ug/L —3-Ofo-b "Kf lo
CC8
184-50-2F
184-50-2F 0
184-50-26 '
184-50-26 D
184-50-2H
184-50-2H 0
184-50-30E
184-50-30E 0
184-50-30E MS
184-50-30E MSO
CCV3:6.0ug/L 	 3-6^3-U fr5E 1
CCS
184-50-3CAB
1S4-50-3CA8 0
184-50-3F
184-50-3F 0
184-50-36
134-50-3G 0
184-50-3H
184-50-3H D
184-50-4CA8
184-50-4CA8 0
CCV4:6.0ug/l 	 3-0^3-1(2. D5€
CCS
184-50-4DE
184-50-40E 0
184-50-4DE MS
184-50-40E HSO
184-50-4F
184-50-4F 0
184-50-46
134-50-46 D
184-50-4H
184-50-4H 0
CCV5=6.0ug/L - 	 	 3_x*o.?/
pro ^ ~" O (A jrty
w WL
184-50-5CA8
184-50-5CA8 0
184-50-580
184-50-5BD D
184-50-5E
184-50-5E D
184-50-5F
                                                                                   150

-------
        Sanole ID         Weight      Dilution
0    184-50-5F D
1    184-50-6CAB
2    184-50-6CAB D
3    CCV6:6.0ug/L
4    CCS
                                                                                                   151

-------
Eleneat:  Hg2
Print Data:  Main+Suppl.
Print: Calib.  Curve
Resarks:
 STANDARDS:  3-023-5
 QC: 3-023-4.1,
INSTRUMENT: 5100
Wavelength: 253.7 Peak
Signal Type: AA
Read Time: 30.0
Sanple Replicates:  1
Standard Replicates:  1
 Calibration Type:  Linear

QC:
Matrix. Check Calculations:
% Difference for Dupls:  No
* Recovery for Spike:  No
Analyst:  0  3TREETER-EDHAROS
Peak -Storaae: Hone
Technique:  MHS           Version: 7.01
Slit: 0.7 Low
Signal Measurement:  Peak Height (5)
Read Delay:  1.0          BOC Tine: 2
FLAME:
Flaae Type:
Oxidant Flow
CALIBRATION:
Solutions
Calib. Blank
Standard 1
Standard 2
Standard 3
Standard 4
Standard 5
Standard o
Calibration
Air
: 10.0 L/nin
1 ID
, i IU Olr\
ISTD i
ISTD 2
ISTD 3
ISTD 4
ISTD 5
ISTO 6
Units: ug/L
Flame Sensor
Fuel Flow: 2
Cone |
1
1
0.2001
0.5001
1.0001
2.0001
5.000',
10.000,'
Sample Units
: On
.0 l/nin

: ug/L
                               Lo:a:ions:
                               Locations:
              ujnc:
                                                                                                                  152

-------
lent File: HG..MEL        Eleient:  Hg?                  Wavelength:  253.
i:  10/21/97.          .     Tiie: 10:09                   Slit:  0.7  L
 File: AB827.DAT         ID/Wt File: AB827.IDW          La»p Current:  0
mique: MHS               Calib. Type: Linear            Energy:  71
.rk 1: STANDARDS: 3-023-5
,rk 2: QC: 3-023-4;o
   ID:  ST  8LK
Seq.  Ho.:  00003    A/S  Pos.:  --    Date:  10/21/97
 icate   1                           Tine:  10:10
  Area  (A-s):  -0.004                Peak Height  (A):  -0.000
 k Corrected  Pk  Height  (A): -0.000
 entration  (ug/L  ):"-0.003

 -zero  performed.
   ID:  STDl:0.2ug/L
Seq.  No.:  00004     A/S  Pos.":  --     Date:  10/21/9'
 icate   1                           Tine: 10:11
  Area  (A-s):  0.170                 Peak Height  (A!:  0.007
 k Corrected  Pk  Height  (A): 0.007
 sntration  (ug/L  ):  0.107

 jard  number  1  apolied.   [0.200]
 slation coefficient:  1.00000       Slope: 0.054o
   ID:  5TD2--0.5uo/L
Sea. No.:  OCOOS    A/£  Pos.:  --     Date:  10/21/9'
 le  abs.  is  greater  than  that of the largest standarc.
 icate   1                           Tine: 10:12
  Area  (A-s):  0.395                 Peak Height (A): 0.013
 < Corrected Pk Height (A):  O.Ole
 antration (ug/L  ):  0.525

 Jard number 2 applied.   [0.500]
 elation  coefficient:  0.99914       Slope: 0.0561
   ID:  STD3=1.0uo/L
Seq. No.: 00006    A/S Pos.:  --     Date:  10/21/97
 le abs.  is greater than that  of  the  largest standard.
 icate  1                          Tine: 10:13
  Area (A-s): 0.878                Peak Height (A): 0.039
 < Corrected Pk Height (A):  0.039
 miration (ug/L  ): 1.073

 fard number 3_applied.   [1.000]
 ilation  coefficient:  0.99824       Slope: 0.0382
   ID:  STD4:2.0ug/L
Seq. No.: 00007    A/S Pos.:  --    Date:  10/21/9'
  e  abs.  is greater than that  of  the  largest standard.
  cate   1                           Ti«e: 10:15
  Area  (A-s):  1.761                Peak Height (A): 0.774
                                                                                                               153

-------
Eleaent File: HG..MEL        Eleunt: Hg2
Date: 10/21/97        -       Tiae:  10:09
Data File: AB827.DAT         ID/HI  File: AB827.IDW
Technique: MHS               lalib.  Type: Linear
Reaark 1: STANDARDS: 3-023-5
Reaark 2: QC= 3-023-4,
                                                          Havelength:  253.
                                                          Slit:  0.7 L
                                                          Laap Current:  0
                                                          Energy:  71
Hg2   ID: ST BLK
                             Seq.  No.:  00003    A/S Pos.: --    Date: 10/21/97
Replicate  1                          Tiie: 10:10
Peak Area (A-s): -0.004               Peak Height (A): -0.000
Blank Corrected Pk Height (A):  -0.000
Concentration (ug/L  ): -0.003

Auto-zero perforaed.
Hg2   ID: STDl=0.2ug/l
                             Seq. No.:  00004     A/S  Pos.:  •-•   Date:.10/21/r
Replicate  1                           Time:  10:11
Peak Area (A-s): 0.170                 Peak Height  (A): 0.007
Blank Corrected Pk Height (A): 0.007
Concentration (ug/L  ): 0.107

Standard number 1 applied.  [0.200]
Correlation coefficient:  1.00000       Slope:  0.034o
 Hg2    ID:  5102=0.5ug/L
                              Seq. No.: 00005    A/£ Pos.:  -     Oats:  10.'21'9'
 Sample  abs.  is  greater  than  that of the largest  standard.
 Replicate   1                           Tine:  10:12
 Peak  Area  (A-s):  0.395                 Peak Height  (A):  0.013
 Blank Corrected Pk  Height  (A): O.Olc
 Concentration (ug/L  ):  0.525

 Standard number 2 applied.   [0.500]
 Correlation coefficient:  0.99914       Slope: 0.036,
 Hg2   ID: 5TD3=1.0ug/L
                              Seq.  No.:  00006    A/S Pos.: --    Date: 10/21/97
 Sarople abs. is greater than that  of  the  largest standar:.
 Replicate  1                          Tine: 10:15
 Peak Area (A-s): 0.878                Peak Height (A): 0.03?
 Blank Corrected Pk Height (A):  0.039
 Concentration (ug/L  ): 1.073

 Standard number 3 applied.  [1.000]
 Correlation coefficient: 0.99824       Slope: 0.038?
 Hg2    ID: STD4:2.0ug/L       Seq.  No.:  00007    A/S Pos.: --    Date: 10/21/9"

 Sasple abs.  is greater than that of the largest standard.
 Replicate   1                           Tine:  10:15
 Peak  Area (A-s):  1.761                 Peak  Height  (A): 0.074
                                                                                                                    154

-------
k.Corrected  Pk  Height  !A): 0.074
entration i.ug/L   ):  1.9*3

oara number  4 applied.   [2.000]
elation coefficient: 0.99947       Slope: 0.0373
  10:  STD5:5.0ug/L       S.eq. No.: 00003    A/S Pos.: --    Date:  10/21/97

le abs.  is greater  than  that of  the  largest standard.
icate  1                          Time: 10:16
 Area (A-s):  4.444                 Peak Height (A): 0..190
< Corrected Pk Height  (A): 0.190
entration (ug/L  ):  5.088

iard number 5 applied.   [5.000]
ilation coefficient:  0.99989       Slope: 0.0379
  ID: STD6:10.0ug/l      Seq.  No.: 00009    A/S Pos.: --    Date:" 10/21/9'

 .e abs. is greater than  that  of  the  Urges: standard.
 .cats  1                          Time:  10:P
 Area (A-s):  5.952                Peak Height (£j: 0.333
 ; Corrected Pk Height  (A):  0.33S
 mtration (ug/L  ): 10.231

 lard number 6 applied.   [10.000]
 ilation coefficient:  0.99389       Sloce: 0.0356
                                                                                                               155

-------
Blank .Corrected  Pk Height  (A): 0.07*
Concentration  i.ug/'l   ):  1.943

Stanoan number  4 applied.   [2.000]
Correlation coefficient: 0.99947       Slope: 0.0373
Hg2   10: 3105=5.Qug/l       5.eq.  No.:  00003     A/S Pos.: -    Date: 10/21/97

Sample abs. is greater than that of  the largest  standard.
Replicate  1                           Tine:  10:16
Peak Area (A-s): 4.444                 Peak Height  (A): 0..190
Blank Corrected Pk Height (A):  0.190
Concentration (ug/L  ):  5.088

Standard nunber 5 applied.  [S.OOO]
Correlation coefficient: 0.99989       Slope:  0.0379
Hg2   ID: STD6:10.0ug/L      Seq. No.: 0000?    A/S Pos.:  --    Date: 10/21/9'

Sample abs. is greater than that of the largest standard. v  .
Reclicate  1                           Tine: 10:1"
Peak Area (A-s): 8.952   '              Peak Height (A):  0.388
Blank Corrected Pk Height (A): 0.33E
Concentration (ug/L   ): 10.231

Standard nunber 6 applied.  [10.000]
Correlation coefficient: 0.99-5S9       Slooe: 0.0386
                                                                                                                        156

-------
ent File: HG..MEL        Eleient: Hg2
:  10/21/97 '              Tine: 10:18
 File:  A6827.DAT         10/Wt File: A8827.IDW
nique:  MHS               Calib. Type: Linear
rk 1:  STANDARDS: 3-023-5
Havelsngth: 253.7
Slit:  0.7 L
laup Current: 0
Energy:  71
M Display Calibration - C:\AAJSER\flflJILES\ELEMENT\HG_.MEL
0.388-,
B"
xx""x
^X^
x
jgf Linear
rgS S4 Corr. Coef.: B. 99989
C70o7s3 Slope: 8,8386
Pr~ Concentration 1B.BBB

4

5j
                                                                                                              157

-------
Element File: H6..HEL        Eleient: Hg2
Date: 10/21/97          .     Tiie: 10:19
Data File: AB827.DAT         I0/Ht File: A8827.IDW
Technique: MHS              .Calib. Type: Linear
Renark 1: STANDARDS: 3-023-5
Renark 2: QC: 3-023-4.Ut
                             Wavelength: 253.7
                             Slit: 0.7 L
                             Laip Current: 0
                             Energy: 71
Hg2   ID: ICV:4.0ug/l
Seq.  No.:  00010    A/S Pos.:  --    Date: 10/21/97
Replicate  1                          Tine: 10:21
Peak Area (A-s): 3.520                Peak Height (A): 0.152
Blank Corrected Pk Height (A):  0.152
Concentration (ug/L  ): 3.941
Hg2   ID:  ICB
Seq.  No.:  00011     A/5  Pos.:  -     Date: 10/21/9'
Reolicate   1                           Time:  10:23
Peak Area  (A-s): 0.008                 Peak Height  (A): 0.000
Blank Corrected Pk Height (A):  0.000
Concentration  (ug/L   ): 0.005
Ha2   ID:  CHECK LO
Seq. No.:  00012     A/S  Pos.:  --     Date:  10/21/9'
 Reolicate   1                           Time:  10:24
 Peak Area  (A-si: 0.163                 Peak  Height  (A!: O.OOt
 Blank  Corrected  Pk Height (A): 0.006
 Concentration  (ug/L   ): 0.166
 Hg2    ID:  43411  M82
Seq. No.: 00013    A/S Pos.:  -     Date:  10/21/9"
 Reolicate   1                           Time:  10:26
 Peak  Area  (A-s):  -0.003                Peak  Height  (Ai:  0.000
 Blank Corrected  Pk  Height  (A): 0.000
 Concentration  (ug/L  ):  0.005
 Hg2    ID:  43411  M82D
 Seq. No.: 00014    A/S Pos.: -   'Date:  10/21/9'
 Replicate  1                          Tine:  10:27 '
 Peak  Area (A-s):  -0.006               Peak Height (A):  -0.000
 Blank Corrected Pk Height (ft): -0.000
 Concentration (ug/L  ): -0.010
 Replicate  1
 Peak Area (A-s): 7.
              s:  10:29  .
           Peak Height .(ft): 0.321  ,
 Blank Correci^trHeignt (A):  0.321
               (ug/L  ): 8.317
 Hg2   ID: 43411 LCS2
 Seq.  No.:  00016    A/S Pos.: -    Date: 10/21/9'
                                                                                                                        158

-------
icate   I                           Ti»e: 10:36
 Area  (A-s).:  4.685                 Peak Height (A): 0.205
(.Corrected  Pk Height (A): 0.205
jntration  (ug/L   ):  5.325
  ID:  43411  ICS2D

.cate   1
 Area  (A-s): 7.480
;  Corrected  Pk Height
intration
  10: 43411 LCS20
                      Seq. No.: 00017    A/S Pos.:  --
                      Seq. No.: 00013    A/S Pos.: --    Date:  10/21/9'
 cate  1                           Tine:  10:41
 Area (A-s): 4.775                 Peak  Height  (A): 0.211
 , Corrected Pk Height (A):  0.211
 .ntration (ug/L  ): 5.473
ID:  184-34-6MS
                         -
                         Seq.  No.:  00019     A/S  Pos.:  --    Date: 10/21/9"
 cate  1                           Time:  10:43
 Area (A-s): 0.085                 Peak  Height  (A):  0.003
  Corrected Pk Height (A):  0.003
 ntration (ug/L  ): 0.081

              MJC.   *& it/-31-41 £C
  ID: 184-84-6.Wftf D      Seq. No.: 00020    A/S Pos.:  --     Date:  10/21/9'

 cate  1                           Time: 10:44
 Area (A-s): 0.07E                 Peak  Height  (A):  0.00!
  Corrected Pk Height (A):  0.003
 ntration (ug/L   ): 0.075
   ID:  184-84-6D
                       Seq.  No.:  00021     A/S  Pos.:  -    Date:  10/21/9'
  cate   1                           Time: 10:45
  Area  (A-s):  0.050                 Peak Height (A): 0.002
   Corrected  Pk  Height  (A): 0.002
  ntration  (ug/L  ):  0.044
   ID:  184-84-6D  D
                       Seq. No.: 00022    A/S Pos.:  --     Date:  10/21/97
  cate   1                           Time: 10:46
  Area  iA-s):  0.042                 Peak Height (A): 0.002
   Corrected Pk  Height  (A):  0.002
  ntration (ug/L  ):  0.039
   ID:  184-84-6D MS
                       Seq. No.: 00023    A/S Pos.:  --     Date:  10/21/97
  cate   1                            Tiie:  10:47
  Area  (A-s):  7.446                 Peak Height (A): 0.314
   Corrected Pk Height (A):  0.3141
                                                                                                                    159

-------
                      / . U . i f
Hg2   ID: 184-84-60 USD       Seq.  No.: 00024"    A/S Pos.: •-    Date:  10/21/97

Replicate  1                            Tine: 10:49
Peak Area (A-s): 7.277                  Peak Height (A): 0.306
Blank Corrected Pk Height  (A):  0.306                                   '    _
Concentration (ug/L   ):  7.947


Hg2   ID: CCV7:6.0ug/L        Seq.  No.: 00025    A/S Pos.: --    Date:  10/21/97

Replicate  1                            Tine: 10:51
Peak Area (A-s): 5.168                  Peak Height (A): 0.220
Blank Corrected Pk Height  (A):  0.220
Concentration (ug/L   ):  5.715


Hg2   ID: CCB                 Seq.  No.: 00026    A/S Pos.: --    Oats:  10/21/9'

Reolicate  1                            Tiie: 10:52
Peak Area (A-s): 0.026                  Peak Height (A): 0.001
Blank Corrected Pk Height  (A):  0.001
Concentration (ug/L   i:  0.018


Hg2   ID: 134-84-6G           Seq.  No.: 00027    A/S Pos.: --    Date:  10/21/97

Replicate  1                            Time: 10:53
Peak Area (A-s): 0.032                  Peak Height (A): 0.001
Blank Corrected Pk Height  (A):  0.001
Concentration (ug/L   ):  0.034

i******!*!*!*,***,*, * *,**•,+, *,»,*, I**! tf^^*,^ ^ i,^*,,,*.*,^*. ,„*„+, t, ft *„ ti ^f.jv^tttf *,*, * I* a *••»*••• *•*•*•* •• I***** »* •*+,** ^tt*,^ m,*t I**,*,
Hg2   ID: 184-84-6G D        Seq.  No.: 00028    A/S Pos.: -    Date:  10/21/9'

Replicate  1                            Time: 10:55
Peak Area (A-s): -0.002                 Peak Height (A):  -0.000
Blank Corrected Pk Height  (A):  -0.000
Concentration (ug/L   ):  -0.003
*~*^**^^~^*****^^~***^***^^^*^**^-*ffi*'*ii,tf~,fr~,ft'*i*'**r-*'****r*r*f*i'***'*'tfi'*'*+t'it+,*t*,f,fitrt,^fr*,f,t,fm*,e,,

Hg2   ID: 184-84-6E           Seq.  He.: 00029    A/S Pos.: -    Date:  10/21/97

Replicate  I                            Tine: 10:56
Peak Area (A-s): 0.132                  Peak Height (A):  0.005
Blank Corrected Pk Height (A):  0.005
Concentration (ug/L   ):  0.138
Hg2    ID:  184-84-6E D
Seq. No.: 00030    A/S  Pos.:  --     Date:  10/21/97
Replicate   1                             Tine:  10:56
Peak Area  (A-s):  0.123                  Peak Height (A):  0.005
Blank  Corrected Pk Height (A): 0.005
Concentration  (ug/L  ): 0.127
                                                                                                                               160

-------
 •  10:  184-84-6F
Seq. No.: 00031    A/S Pos.:  --     Date:  10/21/97
licate   1                           Ti«e: 10:57
k Area  (A-s):  0.001                 Peak Height (A): -0.000
nk Corrected  Pk  Height  (A):  -0.000
:entration (ug/L  ):  -0.003
   ID:  184-84-6F  0        Seq. No.: 00032    A/S Pos.: --    Date: 10/21/9'

.icate   1                          Tine: 10:59
:  Area  (A-s):  0.002                 Peak Height (A): 0:000
ik Corrected Pk Height  (A):  0.000
isntration (ug/L   ):  0.003

              Wo	
   ID:  184-84-7WA8-  _    Seq. No.: 00033    A/S Pos.: -    Date: 10/21/97
                 .   ^VU,.,,x,n fcc

 icate   1               -          Tine: 11:00
  Area  (A-s):- 0.030                 Peak Height (A): 0.001
 k Corrected Pk Height  (A):  0.001
 entration (ug/L   ):  0.031

                    •*> it-swi tt
   ID:  1S4-84-7CWB  D    Seq. No.: 00034    A/S Pos.: --    Date: 10/21/9'

 icate   1                          Time: 11:01
  Area  (A-s):  0.025                 Peak Height (A): 0.001
 k Corrected Pk Height  (A):  0.001
 entration (ug/L   ):  0.018


   10:  184-84-7G          Sea. No.: 00035    A/S Pos.: --    Date: 10/21/97

 icate   1                          Time: 11:02
  Area  (A-s):  -0.005               Peak Height (A): 0.000
 k Corrected Pk Height  (A):  0.000
 Entration (ug/L   ):  0.000


   ID:  184-84-7G  D        Seq. No.: 00036    A/S Pos.: --    Date: 10/21/9'

 icate   1                          Time: 11:05
  Area  (A-s):  -0.024               Peak Height (A): -0.001
 < Corrected Pk Height  (A):  -0.001
 sntration (ug/L   ):  -0.018


   ID:  CCV8:6.0ug/L       Seq. No.: 00037    A/S Pos.: -    Date: 10/21/97

 .cate   1                          Tine: 11:06
  Area  (A-s):  4..679                 Peak Height (A): 0.200
   Corrected Pk Height  (A):  0.200
  ntration (ug/L   ):  5.187
   ID:  CCB
Seq. No.: 00038    A/S Pos.: --  -  Date:  10/21/97
                                                                                                                      161

-------
Peak .Area (A-s): 0.027                 Peak Height  (A): 0.001*
Blank Corrected.Pk Height (A):  0.001
Concentration (ug/L  ): 0.021
Hg2   ID: 184-84-7EF         Seq.  Ho.:  00039     A/S  Pos.:  --    Date: 10/21/9'

Replicate   1                  •         Time:  12:21
Peak Area (A-s): 0.046                 Peak Height  (A):  0.002
Blank Corrected Pk Height (A): 0.002
Concentration  (ug/L   ): 0.044


Hg2   ID: 184-84-7EF  0       Seq.  No.:  00040     A/S  Pos.:  --    Date: 10/21/9'

Replicate   1                           Tine:  12:22
Peak Area (A-s): 0.039                 Peak Height  (A):  0.001
Blank Corrected Pk Height (A): 0.001
Concentration  (ug/L   ): 0.036


Hg2   ID: 184-S4-7EF  HS      Seq.  No.:  00041     A/S  Pos.:  --    Date: 10/21/9'

Replicate   I                           Time:  12:23
Peak Area (A-s): 7.762                 Peak Height  (A):  0.326
Blank Corrected Pk Height (A): 0.326
Concentration  (ug/L   ): 8.442


Hg2   10:  134-84-7EF  USD      See.  No.:  00042     A/S  Pos.:  -    Date: 10/21/9'

 Reolicate   1                           Tine:  12:24
 Peak  Area  (A-s!:  7.774                 Peak  Height  (A):  0.331
 Blank  Corrected  Pk  Height  (A): 0.331
 Concentration (ug/L   ):  8.587


 Hg2   ID:  184-84-7H           Ssq. No.: 00043    A/S Pos.:  -     Date:  10/21/97

 Replicate   1                           Time:  12:25
 Peak  Area  (A-s):  0.141                 Peak Height (A):  0.006
 Blank Corrected Pk  Height  (A): 0.006
 Concentration (ug/L  );  0.148


 Hg2   ID:  184-84-7H D        Seq. No.: 00044    A/5 Pos.:  -    Date:  10/21/9'

 Replicate  1                          Tine: 12:26
 Peak Area (A-s):  0.108                Peak Height  (A): 0.004
 Blank Corrected Pk Height (A):  0.004
 Concentration (ug/L  ):  0.112
 Hg2   ID:  184-34-71
Seq.  No.:  00045    A/S Pos.: -    Date: 10/21/9*
 Replicate   1                •           Tine:  12:27
 Peak Area  (A-s): 0.009                 Peak  Height  (A):  0.000
 Blank Corrected  Pk Height (A): 0.000
                                                                                                                       162

-------
2   10:  184-84-71  D        Seq. No.: 00046    A/S Pos.:  -    Date:  10/21/97

olicate   1                           Tine: 12:28
ak Area  (A-s):  0.004                 Peak Height (A): 0.000
ank Corrected Pk Height  (A): O.OOiX
ncentration (ug/L  ):  0.003
I   ID: CCV9:6.0ug/L       Seq. No.: 00047    A/S Pos.: --    Date:  10/21/97

jlicate  1                          Tine: 12:29
ik Area (A-s):  5.101                Peak Height (A): 0.216
ink Corrected Pk Height (A):  Or216
icentration (ug/L  ):  5.609
 !   ID: CC8       "         Seq.  No.: 00048    A/S Pos.: -    Date:  10/21/9'

 ilicate  1                          Time: 12:33
 ik Area (A-s): -0.011               Peak Height (A): -0.00!
 ink Corrected Pk Height (A):  -0.001
 icentration (ug/L  ): -0.013
 !    ID: 43377 HB1          Seq.  No.:  00049    A/S Pos.: --    Date: 10/21/9"

 ilicate   I                           lime:  12:34
 ik Area (A-si: -0.005                Peak Height  (At:  -0.000
 ink  Corrected Pk Height (A): -0.000
 icsntration (ug/L  ): -O.OOS
 !    ID:  43377 HB1 D        Seq. No.:  00050     A/S  Pos.:  -    Date: 10/21/9'

 ilicate   1                           Time:  12:35
 ik  Area  (A-s):  -0.011                Peak Height  (A):  -0.001
 ink Corrected Pk Height (A): -0.001
 icentration  (ug/L   ): -0.016
 !    ID:  43377  LCS1         Seq. No.: 00051    A/5  Po<_*—*"^Date:  10/21/9

 ilicate   1                  ^^^-^Tj«e:12:36
 ik  Area  (A-s):  7.457^^-^"^     Peak Height (A):  0.322
 ink CorrectedJlMslght  (A): 0.322
 icentratierTT^g/L   ):  8.340
 '    ID:  43377  LCS1          Seq. No.: 00052    A/S Pos.:  -     Date:  10/21/9'

 •licate   1       •                    Tine: 12:41
  k  Area  (A-s):  4.712                 Peak Height (A):  0.204
  nk Corrected  Pk Height  (A): 0.204
  centration  (ug/L   ):  5.278
                                                                                                                       163

-------
ID/Height File: A8828.IDN           Analyst: D.STREETER-EDHARDS
Saiple Volute: 100 iL               Noiinal Height: 1.0 g

  Loc.       Saiple ID         Height       Dilution
0
1
2
3
4
5
6
7
8
9
10
11
12
13
14
15
16
17
18
19
20
21
22
23
24
25
26
27
28
29
30
31
32
33
34
35
36
37
38
39
40
41
42
43
44
45
46
47
48
49
50
isr
1?
13
ST BLANK "X
STDl=0.2ug/L \
STD2=0.5ug/L /
STD3=1.0ug/L (
STD4--2.0ug/L 7-
STD5:5.0ug/L (
STD6=10.0ug/L 1
ICV:4.0ug/L ^__
IC8
CHECK LO
43377 MB2
43377 MB2D
43377 LCS
45377 LCSt-
184-50-6B
184-50-68 D
184-50-680
184-50-6BO 0
184-50-680 MS
184-50-6BD MSD
CCV7--6.0ug/L 	
CCB
184-50-6E
184-50-6E 0
184-50-6FE
184-50-6FE D
184-50-7CA8
184-50-7CAB D
184-50-7E
184-50-7E 0
184-50-7F
.184-50-7F D
CCV8:6.0ug/l 	
CCB
184-50-70
184-50-7D 0
184-50-70 MS
184-50-70 MSO
CCV9:6.0ug/L 	
CCB
42011 Cnl MB
42011 Cnl MSO
42011 LCS
42011 LCSD
170-70-3
170-70-3 D
170-70-3 MS
170-70-3 HSD
CCV:6.0ug/L 	
CCB
43411 MB3
43411 MB 3 D
43411 LCS3
43411 LCS30




3 - 0 93-*? &5£


-3-0a3-r P^











•3-oa3-? ^E











3 -0^3- £* &5tr





3-0>53-ff |Q£ jo








- 3-Cbi3^ £5c






-------
)C.
i'i
isl
)6l
H"'
'8"'.
,0"
.1 '
,2
,3
>4
,5
6
,7
Saaple ID Height Dilution
184-84-580
184-84-5BD 0
184-84-580 HS
184-84-580 USD
CCV10=6.0ug/l —3-023-8 fcS
CCB
184-84-5E
184-84-5E D
184-84-5F
184-84-5F D
184-84-5GF
184-84-5GF D -^
CCVll:6.0ug/L -3-^^"^
CCB
165

-------
Eleaent File:  H6..MEL
Eleient: Hg2
Print Data:  Hain+Suppl.
Print: Calib.  Curve
Reiarks:
 STANDARDS:  3-023-7
 QC: 3-023-8
INSTRUMENT: 5100
Wavelength: 253.7 Peak
Signal Type: AA
Read Tine: 30.0
Satple Replicates: 1
Standard Replicates: 1
FLAME:
Flame Type: Air
Oxidant Flow: 10.0 L/nin
  Calibration Type: Linear
 QC:
 Matrix  Check Calculations:
 \  Difference for Dupls: No
 *  Recovery  for  Spike: No
    Analyst:  D  STREETER-EDHARDS
    Peak Storage:  None
    Technique:  MHS           Version: 7.01
    Slit: 0.7 Lou
    Signal Measureaent:  Peak Height  (5)
    Read Delay: 1.0          BOC Tiie: 2
    Flame Sensor:  On
    Fuel Flow: 2.0 L/ain
CALIBRATION:
Solutions


^.I;L B 1 .» « L
taiiu. dianK
Standard 1
Standard 2
Standard 3
Standard 4
Standard 5
Standard 6
Calibration

i ID
1
1
1 CTf\ ft I V
,5IU OLft
ISTD i
ISTD 2
ISTD 3
ISTD 4
ISTD 5
ISTD 6
Units: ug/L

Cone |
t
(
....... - 1
I
0.2001
0.500!
1.000|
2.000|
5.0001
10.0001
Sanple Units:












ug/L
Locations:
Locations:
Cone:
                                                                                                                  166

-------
«ent File:  H6..HEL        Eleient: Hg2
B:  10/22/97              Tiie: 09:46
a File: AB828.DAT         ID/Nt File: AB828.IDH
hnique: HHS              Calib. Type: Linear
ark 1: STANDARDS:  3-023-7
ark 2: QC:  3-023-8
                                                      Wavelength:  253.7
                                                      Slit:  0.7  L
                                                      Laip Current: 0
                                                      Energy:  71
   10: Seq. 00001

 icate  1
 ; Area (A-s): 0.290
 ik Corrected Pk Height  (A): 0.012

 i-zero perforaed.
                         Seq.  Ho.: 00001    A/S Pos.: -    Date:  10/22/97
                                  Ti»e: 09:46
                                  Peak Height (A): 0.012
                          Seq. No.: 00002    A/S Pos.:  --     Date:  10/22/9^
  ID: Seq. 00002

icate  1
 Area (A-s): 0.020
ik Corrected Pk Height (A):  0.001

-zero performed.
                                   Time: 09:47
                                   Peak Height (A): 0.001
                                                                                                           167

-------
Elenent File: HG..MEL        Eleient: Hg2
Date: 10/22/97               Tiie: 09:48
Data File: AB823.DAT         ID/Ht File: AB823.IDH
Technique: HHS               Calib. Type: Linear
Reiark 1: STANDARDS: 3-023-7
Reiark 2: QC= 3-023-8
                             Wavelength: 253.7
                             Slit: 0.7 I
                             Laip Current: 0
                             Energy: 71
Hg2   10: ST BLANK
Seq.  Ho,:  00003     A/S  Pos.:  --    Date: 10/22/97
Replicate  1                          Tiie: 09:50
Peak Area (A-s): -0.000               Peak Height (A): -0.000
Blank Corrected Pk Height (A):  -0.000

Auto-zero perforaed.
Hg2   ID: STDl:0.2ug/L
Seq.  No.:  00004     A/S  Pos.:  --     Date:  10/22/9'
Replicate   1                           Time:  09:52
Peak Area (A-s): 0.162                 Peak  Height  (A): 0.00'
Blank Corrected Pk Height (A):  0.007

Standard number 1 applied.  [0.200]
Correlation coefficient: 1.00000       Slope:  0.0331
Hg2    10:  ST02:0.5ug/L
Seq. No.: 00005    A/S Pos.:  --     Date:  10/22/97
 Sample  abs.  is greater than that of the largest  standard.
 Replicate   1                           Tine:  09:53
 Peak  Area  (A-s): 0.429                 Peak Height  (A):  0.018^  -.*
 Blank Corrected  Pk Height (A): 0.018                    .s^    Xv &
 Concentration  (ug/L   ): 0.548                                        ^
 Hg2    ID:  STD3:1.0ug/L

 Sasple abs.  is  greater  ttj^rThat of the largest standard.
 Replicate   1        ^^              Tine: 09:54
 Peak  Area  (A-s)xO86                 Peak Height (A):  0.038
 Blank Correefed Pk  Height  (A): 0.038
 ConcejiKeftion (ug/L  ):  1.145
 Hg2   ID:  STD2=0.5ug/L       Seq. No.: 00007    A/S Pos.: --    Date:  10/22/97

 Sample abs. is greater  than  that of the largest standard.
 Replicate   1                          Tiie: 10:01
 Peak Area  (A-s):  0.470                 Peak Height (A): 0.021
 Blank Corrected Pk Height (ft): 0.021
 Concentration (ug/L  ):  0.621

 Standard nuiber 2 applied.   [0.500]
 Correlation coefficient: 0.98455       Slope: 0.0402
                                                                                                                    168

-------
   ID:  ST03:1.0ug/L
Seq. Ho.:  00008     A/S  Pos.: -    Date: 10/22/97
pie abs.  is greater  than  that  of  the largest standard.
licate  1                          Tue: 10:02
k Area (A-s):  0.913                 Peak Height (A): 0.041
nk Corrected Pk Height (A):  0.041
centration (ug/L  ): 1.020

ndard nuiber 3 applied.   [1.000]
relation coefficient: 0.99775       Slope: 0.0409
   ID: STD4:2.0ug/L
Seq. No.: 00009    A/S Pos.:  -     Date:  10/22/97
pie abs. is greater than that of  the  largest standard.
licate  1                          Tine:  10:03
k Area  (A-s): 1.700                Peak  Height  (A): 0.073
nk Corrected Pk Height (A):  0.073
centration (ug/L  ): 1.798

ndard number 4 applied.  [2.000]
relation coefficient: 0.99647      Slope:  0.0378
    ID: STD5:5.0ug/l
Seq. No.: 00010    A/S Pos.:  --    Date:  10/22/97
t>le abs. is greater than that of the largest  standard.
licate  1                           Time:  10:05
k Area  (A-s): 4.214                 Peak Height  (A):  0.180
nk Corrected Pk Height (A): 0.180
:entration (ug/L  ): 4.768

ndard  number 5 applied.  [5.000]
relation coefficient: 0.99923       Slope:  0.0364
    ID:  STD6:10.0ug/L      Seq. No.: 00011    A/S Pos.:  -     Date:  10/22/9-

 Die  abs.  is greater than that of the largest standard.
 licate   1                           Tine: 10:06
 k  Area  (A-s):  8.381                 Peak Height (A):  0.363
 nk Corrected  Pk  Height  (A): 0.363
 :entration  (ug/L  ): 9.993

 idard  number  6 applied.  [10.000]
 relation coefficient: 0.99984       Slope: 0.0364
                                                                                                              169

-------
Eleient File: HG..HEL      Eleient: Hg2
Date: 10/22/97           Tiie: 10:07
Data File: AB828.DAT      ID/Ht File: AB828.IDH
Technique: HHS           Calib. Type: Linear
Reiark 1: STANDARDS: 3-023-7
ReBark 2: QC: 3-023-8
Wavelength: 253.7
Slit: 0.7 L
Laip Current: 0
Energy: 71
          H|  Display Calibration - C;\flfl_USER\flfl.FILES\ELEHEHT\H6_.HEL
                                                     Linear
                                                     Corn.  Coef.:  8.99984
                                                     Slope; B.Q364
                                         Concentration
                                 18.
                                                                                     170

-------
   ID:  ICV:4.0ug/l        Seq. No.: 00012    A/S Pos.: -    Date:  10/22/97

licate   1                           Tiie: 10:12
< Area  (A-s):  3.522                 Peak Height (A): 0.150
ik Corrected  Pk  Height  (A): 0.150
:entration  (ug/L  ):  4.137


   ID:  ICB                Seq. No.: 00013    A/S Pos.: -    Date:  10/22/97

 .icate   1                           Tise: 10:13
 ; Area  (A-s):  0.014                 Peak Height (A): 0.000
 ik Corrected  Pk  Height  (A): 0.000
 :entration  (ug/L  ):  0.003


   ID:  CHECK  LO           Seq. No.: 00014    A/S Pos.: --    Date:  10/22/97

  icate  1                           Tine: 10:15
 . Area (A-s): 0.173                Peak Height (A): 0.007
 ik Corrected  Pk  Height  (A):  0.007
 lentration (ug/L  ):  0.199


   ID:  43377  MB2          Seq. No.: 00015    A/S Pos.: --    Date:  10/22/9'

  icate  1                           Tiie: 10:18
 . Area (A-s): 0.003                Peak Height  (A):  0.000
 ik Corrected Pk Height (A):  0.000
  entration (ug/L  ):  0.003


   ID: 43377 MB2D         Seq.  No.: 00016    A/S Pos.: -    Date: 10/22/97

  icate  1                           Tine:  10:19
  Area  (A-s): 0.005                 Peak Height  (A):  -0.000
  ik Corrected  Pk Height (A): -0.000
  entration (ug/L   ): -0.003


   ID:  43377  LCS          Seq. No.:  00017     A/S  Pos.: -    Date: 10/22/9'

  icate  I                           Tine:  10:20
   Area  (A-s): 4.228                 Peak Height (A):  0.181
  k Corrected  Pk Height (A): 0.181
  entration (ug/L   ): 4.981


   ID:  43377  LCSD        Seq. No.: 00018    A/S Pos.:  --    Date:  10/22/97

  icate  1                           Tiie:  10:22
   Area  (A-s): 4.003                 Peak Height (A):  0.172
  k Corrected  Pk Height (A): 0.172
  entration (ug/L   ): 4.733
    ID:  184-50-68
Seq.  Ho.:  00019     A/S  Pos.: --    Date: 10/22/97
                                                                                                                  171

-------
Concentration {ug/L  ):  4.948
Hg2   ID: 170-70-3           Seq.  No.: 00049    A/S Pos.: -    Date: 10/22/97

Replicate  1                          Tiie: 10:57
Peak Area (A-s): 0.042                Peak Height (A): 0.002
Blank Corrected Pk Height (ft):  0.002
Concentration (ug/L  ): 0.041


Hg2   ID: 170-70-3 D         Seq.  No.: 00050    A/S Pos.: -    Date: 10/22/97

Replicate  1                          Tine: 10:59
Peak Area (A-s): 0.036                Peak Height (A): 0.002
Blank Corrected Pk Height (A):  0.002
Concentration (ug/L  ): 0.041


Hg2   ID: 170-70-3 MS        Seq.  No.: 00051    A/S Pos.: -    Date: 10/22/9'

Replicate  1                          Time: 11:00
Peak Area (A-s): 3.664                Peak Height  (A):  0.16?
Blank Corrected Pk Height (ft):  0.169
Concentration (ug/L  ): 4.65S,


Hg2   ID: 170-70-3 MSD       Seq.  No.: 00052     A/S  Pos.:  --    Date: 10:22''9'

Replicate   1                           Time:  11:01
Peak Area (A-s.l: 3.993                 Peak  Height  (A):  0.1S2
Blank Corrected  Pk Height (A):  0.182
Concentration  (ug/L   ):  5.020


Hg2   ID: CCV=6.0ug/L        Sea. No.:  00053     A/S  Pos.:  --     Date:  10/22/97

Reolicate   1                           Tine:  11:02
 Peak Area  (A-s):  4.793                Peak Height (A):  0.228
Blank Corrected  Pk Height (A): 0.228
Concentration  (ug/L   ):  6.278


 Hg2    ID:  CCB                Seq. No.: 00054    A/S Pos.: --    Date:  10/22/9*

 Replicate   1                          Time: 11:04
 Peak  Area  (A-s):  0.039                Peak Height (A): 0.002
 Blank  Corrected Pk  Height (A): 0.002
 Concentration  (ug/L   ):  0.044
 Hg2   ID: 43411 HB3
Seq.  No.:  00055     A/S  Pos.:  -     Date: 10/22/9*
 Replicate  1                           Tine:  11:05
 Peak Area (A-s): 0.036                 Peak Height  (A):  0.001
 Blank Corrected Pk Height (A):  0.001
 Concentration (ug/L  ): 0.036
                                                                                                                     172

-------
  10:  43411 M83  D         Seq. No.: 00056    A/S Pos.: -    Date:  10/22/97

icate   1                          Tiie: 11:07
 Area  (A-s): 0.028                Peak Height (A): 0.001
k Corrected Pk Height (A):  0.001
entration (ug/L   ):  0.022


  ID:  43411 LCS3         Seq. No.: 00057    A/S Pos.: -    Date:  10/22/97

icate  1                          Ti«e: 11:08
 Area (A-s): 3.908                Peak Height (A): 0.182
k Corrected Pk Height (A):  0.182
sntration (ug/L   ):  5.001


  ID:  43411 LCS3D        Seq. No.: 00058    A/S Pos.: --    Date:  10/22/97

icate  1                          Time: 11:09
 Area (A-s): 3.165                Peak Height (A): 0.176
< Corrected Pk Height (A):  0.176
;ntration  (ug/L   ):  4.846


  ID:  184-34-5BD         Seq. No.: 00059    A/S Pos.: -    Date:  10/22/9'

icate  1                          Time: 11:10
 Area (A-s): 0.050                Peak Height (A): 0.002
< Corrected Pk Height (A):  0.002
:ntration  (ug/L   ):  0.050


  ID:  184-84-5BD D       Seq. No.: 00060    A/S Pos.: --    Date:  10/22/97

icate  1                          Time: 11:11
 Area (A-s): 0.028                Peak Height (A):  0.001
< Corrected Pk Height (A):  0.001
;ntration  (ug/L   ): 0.033


  ID: 184-84-5BD  MS      Seq. No.: 00061    A/S Pos.: --    Date: 10/22/97

 :cate   1                          Tine: 11:11
 Area (A-s): 4.042                Peak Height (A):  0.179
 ( Corrected Pk Height (A):  0.179
 miration  (ug/L   ):  4.926


  ID: 184-84-5BD  HSD     Seq. No.: 00062    ft/S Pos.: --    Date: 10/22/97

 cate  1                          Tine: 11:12
 Area (A-s): 3.862                Peak Height (A):  0.185
  Corrected Pk Height (A):  0.185
 ntration  (ug/L   ):  5.092
  ID: CCV10:6.0ug/L      Seq. No.: 00063    A/S Pos.:  -     Date:  10/22/97
                                                                                                                173

-------
Replicate  1                          Tiie: 11:13
Peak Area (A-s):  5.201                 Peak Height (A): 0.246
Blank Corrected Pk Height (A):  0.246
Concentration (ug/L  ):  6.775
Hg2   ID: CCB                Seq.  No.:  00064    A/S Pos.: -    Date: 10/22/97

Replicate  1                           Tine:  11:14
Peak Area (A-s): 0.075                 Peak Height (A): 0.003
Blank Corrected Pk Height (A): 0.003
Concentration (ug/L  ): 0.080


Hg2   ID: 184-84-5E          Seq.  No.:  00065    A/S Pos.: --    Date: 10/22/97

Replicate  1                           Tine:  11:15
Peak Area (A-s): 0.043                 Peak Height (A): 0.002
Blank Corrected Pk Height (A): 0.002
Concentration (ug/L  ): 0.041


Hg2   ID: 184-84-5E D        Seq.  No.:  00066    A/S Pos.: -    Date: 10/22/97

Replicate  1                           Tine:  11:16
Peak Area (A-s): 0.033                 Peak  Height  (A):  0.001
Blank Corrected Pk Height (A): 0.001
Concentration (ug/L  ): 0.036


Hg2   ID: 184-84-5F           Seq.  No.:  00067     A/S Pos.: --    Date: 10/22/97

Replicate   1                           Tine:  11:16
Peak Area (A-s): 0.033                 Peak  Height  (A):  0.001
Blank Corrected Pk Height  (A): 0.001
Concentration  (ug/L   ):  0.030


Hg2    ID: 184-84-5F  D         Seq. No.: 00068    A/S Pos.:  -    Date:  10/22/97

 Replicate   1                           Time: 11:17
 Peak Area  (A-s):  0.030                Peak Height  (A):  0.001
 Blank  Corrected Pk  Height  (A): 0.001
 Concentration  (ug/L   ):  0.025


 Hg2    ID:  184-84-5GF         Seq. No.: 00069    A/S Pos.:  --    Date:  10/22/97

 Replicate  1                          Tine: 11:18
 Peak Area (A-s): 0.045                Peak  Height (A):  0.002
 Blank  Corrected Pk Height (A):  0.002
 Concentration (ug/L  ):  0.044
 Hg2   ID: 184-84-56F D
Seq.  No.:  00070    A/S Pos.: --    Date: 10/22/97
 Replicate  1                           Tine:  11:19
 Peak Area (A-s): 0.043                 Peak  Height  (A): 0.002
 Blank Corrected Pk Height (A): 0.002
                                                                                                                        174

-------
ncentration  (ug/L   ): 0.041
2   10:  CCVll:6.0ug/L      Seq. Ho.: 00071    A/S  Pos.: --    Date:  10/22/97

plicate  1                          Tiie: 11:19
ak Area (A-s):  4.696                 Peak Height  (A): 0.236
ank Corrected Pk Height  (A): 0.236
ncentration (ug/L  ):  6.485
2   ID: CCB                Seq. Ho.: 00072    A/'S Pos.: -    Date: 10/22/97

Dlicate  1                          Tine: 11:20
ak Area (A-s): 0.046                Peak Height (A):  0.002
ank Corrected Pk Height (A):  0.002
ncentration (ug/L  ):  0.047
                                                                                                                175

-------

-------
     APPENDIX D




COMPUTER SUMMARIES

-------
        Appendix D.I




     Computer Summaries




Baghouse Inlet - Method 23 & 29

-------
Summary of Stack Gas Parameters and Test Results
As-pHfH-TVt-Atrr "8" - Gary, North Carolina
US EPA Test Method 23 - PCDD / PCDF
Baghouse Inlet
Page 1 of 6




Y
AH
Pbar
vm
Tm
Pstatic
Ts
vte
CO2
02
N2
CP
Ap1*
e
Dn

An
Vm(std)
Vm(sld)
PS
Bw,
Vwstd
1-B™
Md
Ms
Vs
A
Qa
Q.
Qs(cmm)
I
RUN NUMBER
RUN DATE
RUN TIME
MEASURED DATA
Meter Box Correction Factor
Avg Meter Orifice Pressure, in. H2O
Barometric Pressure, inches Hg
Sample Volume, ft3
Average Meter Temperature, °F
Stack Static Pressure, inches H2O
Average Stack Temperature, °F
Condensate Collected, ml
Carbon Dioxide content, % by volume
Oxygen content, % by volume
Nitrogen content, % by volume
Pilot Tube Coefficient
Average Square Root Dp, (in. H2O)iy2
Sample Run Duration, minutes
Nozzle Diameter, inches
CALCULATED DATA
Nozzle Area, ft2
Standard Meter Volume, dscf
Standard Meter Volume, dscm
Stack Pressure, inches Hg
Moisture, % by volume
Standard Water Vapor Volume, ft3
Dry Mole Fraction
Molecular Weight (d.b.), Ib/lb-mole
Molecular Weight (w.b.), Ib/lb-mole
Stack Gas Velocity, ft/s
Stack Area, ft2
Stack Gas Volumetric flow, acfm
Stack Gas Volumetric flow, dscfm
Stack Gas Volumetric flow, dscmm
Isokinetic Sampling Ratio, %
R-M23-I-1
8/27/97
0940-1227

1.021
1.21
29.80
58.263
96
-1.8
308
510.5
5.2
13.8
81.0
0.84
0.6901
96
0.257

0.00036
56.399
1.597
29.67
29.9
24.029
0.701
29.38
25.98
49.5
16.20
48,074
22,981
650.7
115.0
R-M234-2
8/28/97
0908-1428

1.021
0.286
29.60
53.015
96
-1.8
306
414.9
5.2
13.1
81.7
0.84
0.6755
170
0.194

0.00021
50.885
1.441
29.47
27.7
19.529
0.723
29.36
26.21
48.3
16.20
46,957
23,027
652.1
102.6
R-M23-I-3
8/29/37
0818-1413

1.021
0.396
29.60
83.709
93
-1.8
290
393.0
4.0
15.2
80.8
0.84
0.7133
240
0.194

0.00021
80.735
2.286
29.47
18.6
18.499
0.814
29.25
27.15
49.6
16.20
48,211
27,178
769.6
97.7
Average of
1st and 2nd
Test Run

1.021
0.75
29.70
55.639
96
-1.8
307
462.7
5.2
13.5
81.4
0.84
0.6828
133
0.226

0.00028
53.642
1.519
29.57
28.8
21.779
0.712
29.37
26.09
48.9
16.20
47,515
23,004
651.4
108.8

-------
Summary of Stack Gas Parameters and Test Results
foptttu- 7*Aur"«" • Gary, North Carolina
US EPA Test Method 23 - PCDD / PCDF
Baghouse Inlet
Page 2 of 6






(ng)
(ng/dscm)
(M9/hr)

(ng)
(ng/dscm)
(pg/hr)

(ng)
(ng/dscm)
(pg/hr)

(ng)
(ng/dscm)
(pg/hr)

(ng)
(ng/dscm)
(pg/hr)

(ng)
(ng/dscm)
(pg/hr)
RUN NUMBER
RUN DATE
RUN TIME
EMISSIONS DATA
DIOXINS:
2378 TCDD
Catch, ng
Concentration, ng/dscm, as measured
Emission Rate, pg/hr
Total TCDD
Catch, ng
Concentration, ng/dscm, as measured
Emission Rate, pg/hr
12379PeCPP
Catch, ng
Concentration, ng/dscm, as measured
Emission Rate, pg/hr
Total PeCDD
Catch, ng
Concentration, ng/dscm, as measured
Emission Rate, pg/hr
123478 HxCDD
Catch, ng
Concentration, ng/dscm, as measured
Emission Rate, pg/hr
123678 HxCDD
Catch, ng
Concentration, ng/dscm, as measured
Emission Rate, pg/hr
R-M23-I-1
8/27/97
0940-1227



ND
ND
ND

ND
ND
ND

ND
ND
ND

ND
ND
ND

ND
ND
ND

ND
ND
ND
R-M23-I-2
8/28/97
0908-1428



ND
ND
ND

ND
ND
ND

ND
ND
ND

ND
ND
ND

ND
ND
ND

ND
ND
ND
R-M23-I-3
8/29/97
0818-1413



ND
ND
ND

ND
ND
ND

ND
ND
ND

ND
ND
ND

ND
ND
ND

ND
ND
ND
Avenge of
1st and 2nd
Test run



ND
ND
ND

ND
ND
ND

ND
ND
ND

ND
ND
ND

ND
ND
ND

ND
ND
ND
()  Not Detected.  Value shown is the detection limit for that sample.
{}  Estimated Maximum Possible Concentration.

-------
Summary of Stack Gas Parameters and
Test Results


.?:?*4tr TiAm "g"i - Gary, North Carolina
US EPA Test Method 23 - PCDO / PCDF







RUN NUMBER
RUN DATE
RUN TIME
Baghouse Inlet
Page 3 of 6
R-M23-I-1
8/27/97
0940-1227


R-M23-I-2
8/28/97
0908-1428


R-M23-I-3
8/29/97
0818-1413


Avenge of
1st and 2nd
Test Run
EMISSIONS DATA -Continued


(ng)
(ng/dscm)
(pg/hr)

(ng)
(ng/dscm)
(pg/hr)

(ng)
(ng/dscm)
(pg/hr)

(ng)
(ng/dscm)
(pg/hr)

(ng)
(ng/dscm)
(pg/hr)

(ng)
(ng/dscm)
(pg/hr)
DIOXINS - Continued
123789 HxCDD
Catch, ng
Concentration, ng/dscm,
Emission Rate, pg/hr
Total HxCDD
Catch, ng
Concentration, ng/dscm,
Emission Rate, pg/hr
1234678 HpCDD
Catch, ng
Concentration, ng/dscm,
Emission Rate, pg/hr
Total HpCDD
Catch, ng
Concentration, ng/dscm,
Emission Rate, pg/hr
1 2346789 OCPD
Catch, ng
Concentration, ng/dscm,
Emission Rate, pg/hr
Total PCDD
Catch, ng
Concentration, ng/dscm,
Emission Rate, pg/hr


ND
as measured ND
ND

ND
as measured ND
ND

ND
as measured ND
ND

{0.350}
as measured {0.219}
{8.56}

9.70
as measured 6.07
237

{10.1}
as measured {6.29}
{246}

-
ND
ND
ND

ND
ND
ND

ND
ND
ND

ND
ND
ND

8.20
5.69
223

8.20
5.69
223


ND
ND
ND

0.0200
0.00875
0.404

0.140
0.0612
2.83

0.340
0.149
6.87

16.2
7.09
327

16.6
7.24
334


ND
ND
ND

ND
ND
ND

ND
ND
ND

{0.175}
{0.110}
{4.28}

8.95
5.88
230

{9.13}
{5.99}
{234}
() Not Detected.  Value shown is the detection limit for that sample.
{} Estimated Maximum Possible Concentration.

-------
Summary of Stack Gas Parameters and
Test Results
fcpHter Tt/fcur "B '•'- Gary, North Carolina
US EPA Test Method 23 - PCDD /







RUN NUMBER
RUN DATE
RUN TIME
Baghouse Inlet
Page 4 of 6
R-M23-I-1
8/27/97
0940-1227
PCDF


R-M23-I-2
8/28/97
0908-1428



R-M23-I-3
8/29/97
0818-1413



Average of
1st and 2nd
Test Run
EMISSIONS DATA - Continued


(ng)
(ng/dscm)
(ug/hr)

(ng)
(ng/dscm)
(ug/hr)

(ng)
(ng/dscm)
(ug/hr)

(ng)
(ng/dscm)
(ug/hr)

(ng)
(ng/dscm)
(ug/hr)

(ng)
(ng/dscm)
(ug/hr)
FURANS
2378 TCDF
Catch, ng
Concentration, ng/dscm,
Emission Rate, ug/hr
Total TCDF
Catch, ng
Concentration, ng/dscm,
Emission Rate, ug/hr
12378 PeCDF
Catch, ng
Concentration, ng/dscm,
Emission Rate, ug/hr
23478 PeCDF
Catch, ng
Concentration, ng/dscm,
Emission Rate, ug/hr
Total PeCDF
Catch, ng
Concentration, ng/dscm
Emission Rate, ug/hr
1 23478 HxCDF
Catch, ng
Concentration, ng/dscm
Emission Rate, ug/hr


ND
as measured ND
ND

{0.180}
as measured {0.113}
{4.40}

ND
as measured ND
ND

ND
as measured ND
ND

0.470
as measured 0.294
11.5

ND
as measured ND
ND


ND
ND
ND

0.170
0.118
4.62

ND
ND
ND

ND
ND
ND

0.330
0.229
8.96

ND
ND
ND


ND
ND
ND

0.0100
0.00437
0.202

ND
ND
ND

ND
ND
ND

{0.0100}
{0.00437}
{0.202}

0.0200
0.00875
0.404


ND
ND
ND

{0.175}
{0.115}
{4.51}

ND
ND
ND

ND
ND
ND

0.400
0.262
10.2

ND
ND
ND
()  Not Detected. Value shown is the detection limit for that sample.
{}  Estimated Maximum Possible Concentration.

-------
ftspnAtrTiAMT "B" - Gary, North Carolina
US EPA Test Method 23 - PCDD / PCDF
Baghouse Inlet







(ng)
(ng/dscm)
(pg/hr)

(ng)
(ng/dscm)
(pg/hr)

(ng)
(ng/dscm)
(pg/hr)

(ng)
(ng/dscm)
(pg/hr)

(ng)
(ng/dscm)
(pg/hr)

(ng)
(ng/dscm)
(|jg/hr)
Page
RUN NUMBER
RUN DATE
RUN TIME
EMISSIONS DATA - Continued
Furans - Continued
123678 HxCDF
Catch, ng
Concentration, ng/dscm, as measured
Emission Rate, pg/hr
234678 HxCDF
Catch, ng
Concentration, ng/dscm, as measured
Emission Rate, pg/hr
123789 HxCDF
Catch, ng
Concentration, ng/dscm, as measured
Emission Rate, pg/hr
Total HxCDF
Catch, ng
Concentration, ng/dscm, as measured
Emission Rate, pg/hr
1 234678 HpCDF
Catch, ng
Concentration, ng/dscm, as measured
Emission Rate, pg/hr
1234789 HpCDF
Catch, ng
Concentration, ng/dscm, as measured
Emission Rate, pg/hr
5 of 6
R-M23-I-1
8/27/97
0340-1227



ND
ND
ND

ND
ND
ND

ND
ND
ND

ND
ND
ND

ND
ND
ND

ND
ND
ND

R-M23-I-2
8/28/97
0908-1428



ND
ND
ND

ND
ND
ND

ND
ND
ND

ND
. ND
ND

ND
ND
ND

ND
ND
ND

R-M23-I-3
8/29/97
0818-1413



ND
ND
ND

{0.00600}
{0.00262}
{0.121}

ND
ND
ND

0.0300
0.0131
0.606

0.0400
0.0175
0.808

ND
ND
ND

Average of
1st and 2nd
Test run



ND
ND
ND

ND
ND
ND

ND
ND
ND

ND
ND
ND

ND
ND
ND

ND
ND
ND
()  Not Detected. Value shown is the detection limit for that sample.
{}  Estimated Maximum Possible Concentration.

-------
Summary of Stack Gas Parameters and Test Results
A&H&.T TLA™ "8" , - Gary, North Carolina
US EPA Test Method 23 - PCDD / PCDF
Baghouse Inlet
Page 6 of 6






(ng)
(ng/dscm)
(pg/hr)

(ng)
(ng/dscm)
(pg/hr)

(ng)
(ng/dscm)
(pg/hr)

(ng)
(ng/dscm)
(pg/hr)
RUN NUMBER
RUN DATE
RUN TIME
EMISSIONS DATA - Continued
Furans - Continued
Total HpCDF
Catch, ng
Concentration, ng/dscm, as measured
Emission Rate, (jg/hr
1 2346789 OCDF
Catch, ng
Concentration, ng/dscm, as measured
Emission Rate, pg/hr
Total PCDF
Catch, ng
Concentration, ng/dscm, as measured
Emission Rate, pg/hr
Total PCDD + PCDF
Catch, ng
Concentration, ng/dscm, as measured
Emission Rate, pg/hr
R-M23-I-1
8/27/97
0940-1227



ND
ND
ND

ND
ND
ND

{0.650}
{0.407}
{15.9}

{10.7}
{6.70}
{262}
R-M23-I-2
8/28M7
0908-1428



{0.260}
{0.180}
{7.06}

ND
ND
ND

{0.760}
{0.527}
{20.6}

{8.96}
{6.22}
{243}
R-M23-I-3
8/29/97
0818-1413



0.0400
0.0175
0.808

ND
ND
ND

{0.0900}
{0.0394}
{1.82}

{16.7}
{7.28}
{336}
Avenge of
1st and 2nd
Test run



{0.130}
{0.0902}
{3.53}

ND
ND
ND

{0.705}
{0.467}
{18.3}

{9.83}
{6.46}
{252}
()  Not Detected.  Value shown is the detection limit for that sample.
{}  Estimated Maximum Possible Concentration.

-------
PCDD/PCDF Corrected Stack Gas Concentrations and 2378 TCDD Toxic Equivalent Concentrations
                        AynAtf ~Putntr « A"    . Garner, North Carolina
                          US EPA Test Method 23 - PCDD/PCDF
                                   Baghouse Inlet

RUN NUMBER
RUN DATE
RUN TIME
DIOXINS:
2378 TCDD
Total TCDD
12378 PeCDD
Total PeCDD
123478 HxCDD
1 23678 HxCDD
123789 HxCDD
Total HxCDD
1 234678 HpCDD
Total HpCDD
12346789 OCDD
Total PCDD
FURANS:
2378 TCDF
Total TCDF
12378 PeCDF
23478 PeCDF
Total PeCDF
123478 HxCDF
123678 HxCDF
234678 HxCDF
123789 HxCDF
Total HxCOF
1234678 HpCDF
1 234789 HpCDF
Total HpCDF
1 2346789 OCDF
Total PCDF
Total PCDD + PCDF
CONCENTRATION
(ng/dscmm, adjusted to 7% O2)
R-M23-I-1 R-M23-I-2 R-M23-I-3
08/27/97 08/28/97 08/29/97
0940-1227 0908-1428 0818-1413

ND NO ND
ND ND ND
ND ND ND
ND ND ND
ND ND ND
ND ND ND
ND ND ND
ND ND 0.0213
ND ND 0.149
{0.429} ND 0.363
11.9 10.1 17.3
{12.3} 10.1 17.7

ND ND ND
{0.221} 0.210 0.0107
ND ND ND
ND ND ND
0.576 0.408 {0.0107}
ND ND 0.021
ND ND ND
ND ND {0.00640}
ND ND ND
ND ND 0.0320
ND ND 0.0427
ND ND ND
ND {0.322} 0.0427
ND ND ND
{0.797} {0.940} {0.0960}
{13.1} {11.1} {178}
Average
of 1st & 2nd
Run

ND
ND
ND
ND
ND
ND
ND
ND
ND
{0.215}
11.0
{11.2}

ND
{0.215}
ND
ND
0.492
ND
ND
ND
ND
ND
ND
ND
{0.161}
ND
{0.868}
{12.1}
2378-TCDD
Toxic
Equivalent
Factor

1.000

0.500

0.100
0.100
0.100

0.010

0.001


0.100

0.050
0.500

0.100
0.100
0.100
0.100

0.010
0.010

0.001


2378 TOXIC EQUIVALENCIES
(ng/dscmm, adjusted to 7% O2)
R-M23-I-1 R-M23-I-2 R-M23-I-3
8/27/97 8/28/97 8/29/97
0940-1227 0908-1428 0818-1413

ND ND ND
"
ND ND ND

ND ND ND
ND ND ND
ND ND ND

ND ND 0.001

0.0119 0.0101 0.0173
0.0119 0.0101 0.0188

ND ND ND

ND ND ND
ND ND ND

ND ND 0.00213
ND ND ND
ND ND {0.000640}
ND ND ND

ND ND 0.000427
ND ND ND

ND ND ND
ND ND {0.00320}
0.0119 0.0101 {0.0220}
Average
of 1st & 2nd
Run

ND

ND

ND
ND
ND

ND

0.0110
0.0110

ND

ND
ND

ND
ND
ND
ND

ND
ND

ND
ND
0.0110

-------
Summary of Stack Gas Parameters and Test Results
US EPA EMC Asphalt Concrete Emissions Testing • ftsmdu VUt,
US EPA Test Method 29 - Multiple Metals
Baghouse Inlet
Page 1 of 4




y
AH
Pbar
vm
Tm
•static
Ts
V,c
CO2
02
IM2
Vp
Ap
e
Dn

An
Vm(std)cf
Vjn(std) cm
Qm
PS
Bws
VW5td
1-BWS
Md
Ms
vs
A
Qa
Qscfm
Qscmm
I
RUN NUMBER
RUN DATE
RUN TIME
MEASURED DATA
Meter Box Correction Factor
Avg Meter Orifice Pressure, in. H20
Barometric Pressure, inches Hg
Sample Volume, ft3
Average Meter Temperature, °F
Stack Static Pressure, inches H2O
Average Stack Temperature, °F
Condensate Collected, ml
Carbon Dioxide content, % by volume
Oxygen content, % by volume
Nitrogen content, % by volume
Pilot Tube Coefficient
Average Square Root Ap, (in. H2O)1/2
Sample Run Duration, minutes
Nozzle Diameter, inches
CALCULATED DATA
Nozzle Area, ft2
Standard Meter Volume, ft3
Standard Meter Volume, m3
Average Sampling Rate, dscfm
Stack Pressure, inches Hg
Moisture, % by volume
Standard Water Vapor Volume, ft3
Dry Mole Fraction
Molecular Weight (d.b.), Ib/lb-mole
Molecular Weight (w.b.), Ib/lb-mole
Stack Gas Velocity, ft/s
Stack Area, ft2
Stack Gas Volumetric flow, acfm
Stack Gas Volumetric flow, dscfm
Stack Gas Volumetric flow, dscmm
Isokinetic Sampling Ratio, %
R-M29-I-1
«/27/97
-1000—1200

1.016
1.24
29.80
52.232
101
-1.8
304
422.5
4.6
14.2
81.2
0.84
0.6972
87
0.256

0.000357
49.883
1.413
0.573
29.67
28.5
19.887
0.715
29.30
26.08
49.7
16.20
48,345
23,687
671
109.7
R-M29-I-2
8/28/97
1019-1427

1.016
OJ298
29.60
64.379
102
-1.8
309
485.0
5.2
13.1
81.7
0.84
0.6977
200
0.194

0.000205
60.783
1.721
0.304
29.47
27.3
22.829
0.727
29.36
26.26
49.9
16.20
48,535
23,865
676
100.5
itr "B"
R-M29-I-3
8/29/97
0819-1403

1.016
0.400
29.60
85.398
96
-1.8
289
403.9
4.0
15.2
80.8
0.84
0.7185
240
0.196

0.000210
81.522
2.308
0.340
29.47
18.9
19.012
0.811
29.25
27.12
49.9
16.20
48,550
27,325
774
96.1

Average of
1st and 2nd
Test Runs

1.016
0.771
29.700
58.306
101.622
-1.800
306.083
453.750
4.900
13.650
81.450
0.840
0.697
143.500
0.225

0.000281
55.333
1.567
0.439
29.57
27.9
21.358
0.721
29.33
26.17
49.8
16.20
48,440
23,776
673
105.1

-------
Summary of Stack Gas Parameters and Test Results
US EPA EMC Asphalt Concrete Emissions Testing • KsryQiT Pt*
-------
Summary of Stack Gas Parameters and Test Results
US EPA EMC Asphalt Concrete Emissions Testing - Aspn*a fa
US EPA Test Method 29 - Multiple Metals
Baghouse Inlet






pg
pg/dscm
pg/dscm at 7%
g/hr

pg
pg/dscm
pg/dscm at 7%
g/hr

pg
pg/dscm
pg/dscm at 7%
g/hr

pg
pg/dscm
pg/dscm at 7%
g/hr

pg
pg/dscm
pg/dscm at 7%
g/hr

pg
pg/dscm
pg/dscm at 7%
g/hr

RUN NUMBER
RUN DATE
RUN TIME
EMISSIONS DATA -Continued
Chromium
Target Catch, pg
Concentration, pg/dscm
Concentration, pg/dscm at 7% O2
Emission Rate, g/hr
Colbalt
Target Catch, pg
Concentration, pg/dscm
Concentration, pg/dscm at 7% O2
Emission Rate, g/hr
Copper
Target Catch, pg
Concentration, pg/dscm
Concentration, pg/dscm at 7% O2
Emission Rate, g/hr
Lead
Target Catch, pg
Concentration, pg/dscm
Concentration, pg/dscm at 7% O2
Emission Rate, g/hr
Manganese
Target Catch, pg
Concentration, pg/dscm
Concentration, pg/dscm at 7% O2
Emission Rate, g/hr
Mercury
Target Catch, pg
Concentration, pg/dscm
Concentration, pg/dscm at 7% O2
Emission Rate, g/hr
Page 3 of 4
R-M29-I-1
8/27/97
-1000-1200


95.8
67.8
141
2.73

63.2
44.7
92.8
1.80

613
434
900
17.5

85.3
60.4
125
2.43

2,471
1,750
3,630
70.4

ND
ND
ND
ND

R-M29-I-2
8/28/97
1019-1427


88.3
"51.3
91.4
2.08

55.1
32.0
57.0
1.30

660
384
684
15.6

83.1
48.3
86.0
1.96

2,336
1,357
2,418
55.0

ND
ND
ND
ND
4<«r "g"

R-M29-I-3
8/29/97
0819-1403


76.8
33.3
81.2
1.55

45.5
19.7
48.1
0.915

607
263
641
12.2

82.7
35.8
87.4
1.66

2,251
975
2,377
45.3

ND
ND
ND
ND


Average of
1st and 2nd
Test Runs


92.1
59.6
116
2.41

59.2
38.4
74.9
1.55

636
409
792
16.5

84.2
54.3
106
2.19

2,404
1,553
3,024
62.7

ND
ND
ND
ND

-------

Summary of Stack Gas Parameters and Test Results
US EPA EMC Asphalt Concrete Emissions Testing • f,s,?miLr v-v .4*-; "3"
US EPA Test Method 29 - Multiple Metals
Baghouse Inlet






pg
pg/dscm
pg/dscm at 7%
g/hr

H9
pg/dscm
pg/dscm at 7%
g/hr

MS
pg/dscm
pg/dscm at 7%
g/hr

P9
pg/dscm
pg/dscm at 7%
g/hr

P9
pg/dscm
pg/dscm at 7%
g/hr

M9
pg/dscm
pg/dscm at 7%
g/hr

fl(W NUMBER
RUN DATE
RUN TIME
EMISSIONS DATA - Continued
Nickel
Target Catch, pg
Concentration, pg/dscm
Concentration, pg/dscm at 7% O2
Emission Rate, g/hr
Phosphorus
Target Catch, pg
Concentration, pg/dscm
Concentration, pg/dscm at 7% O2
Emission Rate, g/hr
Silver
Target Catch, pg
Concentration, pg/dscm
Concentration, pg/dscm at 7% O2
Emission Rate, g/hr
Selenium
Target Catch, pg
Concentration, pg/dscm
Concentration, pg/dscm at 7% O2
Emission Rate, g/hr
Thallium
Target Catch, pg
Concentration, pg/dscm
Concentration, pg/dscm at 7% O2
Emission Rate, g/hr
Zinc
Target Catch, pg
Concentration, pg/dscm
Concentration, pg/dscm at 7% O2
Emission Rate, g/hr
Page 4 of 4
R-M29-I-1
8/27/97
-1000-1200


59.0
4^.7
86.6
1.68

4,250
3,009
6,242
121

1.20
0.850
1.76
0.0342

ND
ND
ND
ND

12.2
8.64
17.9
0.348

761
539
1,118
21.7

R-M29-I-2
8/28/97
1019-1427


58.4
33.9
60.5
1.38

3,874
2,251
4,011
91.3

1.00
0.581
1.04
0.0236

0.396
0.230
0.410
0.00933

8.58
4.98
8.88
0.202

683
397
707
16.1

R-M29-I-3
8/29/97
0819-1403


50.3
21.8
53.1
1.01

5,010
2,170
5,292
101

0.671
0.291
0.709
0.0135

ND
ND
ND
ND

2.08
0.901
2.20
0.0418

553
239
584
11.1

Average o
1st and 2,
Test Rom


5
3
7.'
1

4,0'
2,6:
5,1:
1t

1.1
0,71
1.4
0.026

0,19
0.11
0.20.
0.0046!

10.3S
6.81
13.4C
Q27£

722
468
913
18.9

-------

-------
          Appendix D.2




       Computer Summaries




Baghouse Outlet - Method 9, 23 & 29

-------

-------
                         Date:
                    Start Time:
                    Stop Time:
8/29/97
 0923
 1023
   Baghouse Outlet
Run Number: O-M9-3B
Net Run
Time,
minutes
0.25
0.50
0.75
1.00
1.25
1.50
1.75
2.00
2.25
2.50
2.75
3.00
3.25
3.50
3.75
4.00
4.25
4.50
4.75
5.00
5.25
5.50
5.75
6.00
6.25
6.50
6.75
7.00
7.25
7.50
7.75
8.00
8.25
8.50
8.75
9.00
9.25
9.50
9.75
10.00
10.25
10.50
10.75
11.00
11.25
11.50
11.75
12.00
HIGT
six-minute
rolling averages
percent opacity,
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
1.25
1.46
.46
.46
.25
.04
.25
.25
.25
.25
.25
.25
.25
.25
1.25
1.25
1.25
1.04
1.25
1.25
1.25
1.67
1.67
1.67
1.46
Net Run
Time,
minutes
12.25
12.50
12.75
13.00
13.25
13.50
13.75
14.00
14.25
14.50
14.75
15.00
15.25
15.50
15.75
16.00
16.25
16.50
16.75
17.00
17.25
17.50
17.75
18.00
18.25
18.50
18.75
19.00
19.25
19.50
19.75
20.00
20.25
20.50
20.75
21.00
21.25
21.50
21.75
22.00
22.25
22.50
22.75
23.00
23.25
23.50
23.75
24.00
six-minute
rolling averages
percent opacity,
.46
.46
.46
.67
.67
.46
.46
.67
.46
.46
.46
.46
.67
.67
.88
2.08
2.08
1.88
1.88
1.88
1.46
1.46
1.46
1.46
1.30
1.30
1.30
1.09
1.09
1.09
1.09
1.30
1.30
1.52
1.74
1.74
1.52
1.96
1.52
1.30
1.30
1.30
1.30
1.30
1.30
1.30
1.36
1.36
Net Run
Time,
minutes
24.25
24.50
24.75
25.00
25.25
25.50
25.75
26.00
26.25
26.50
26.75
27.00
27.25
27.50
27.75
28.00
28.25
28.50
28.75
29.00
29.25
29.50
29.75
30.00
30.25
30.50
30.75
31.00
31.25
31.50
31.75
32.00
32.25
32.50
32.75
33.00
33.25
33.50
33.75
34.00
34.25
34.50
34.75
35.00
35.25
35.50
35.75
36.00
six-minute
rolling averages
percent opacity,
1.30
1.30
.52
.52
.52
.52
.96
.52
.52
.30
.09
.09
.09
0.65
0.65
0.65
0.68
0.68
0.68
0.68
0.68
0.68
0.65
0.65
0.65
0.65
0.43
0.43
0.43
0.43
0.00
0.00
0.22
0.22
0.22
0.22
0.22
0.22
0.22
0.22
0.63
0.63
0.63
0.63
0.83
0.83
0.83
1.04
[ESt SlX-MINUTE BLOCK AVERAGE - 1.46 AVE
Net Run
Time,
minutes
36.25
36.50
36.75
37.00
37.25
37.50
37.75
38.00
38.25
38.50
38.75
39.00
39.25
39.50
39.75
40.00
40.25
40.50
40.75
41.00
41.25
41.50
41.75
42.00
42.25
42.50
42.75
43.00
43.25
43.50
43.75
44.00
44.25
44.50
44.75
45.00
45.25
45.50
45.75
46.00
46.25
46.50
46.75
47.00
47.25
47.50
47.75
48.00
RAGEO
six-minute
rolling averages
percent opacity,
1.04
.04
.04
.04
.25
.25
.25
.46
.25
.25
•25
.25
.25
.25
.25
.25
0.83
0.83
1.04
1.25
1.04
1.04
1.04
0.83
0.83
0.83
1.04
1.04
0.83
0.83
0.83
0.63
0.63
0.63
0.63
0.63
0.63
0.63
0.83
0.83
0.83
0.83
0.63
0.42
0.42
0.42
0.42
0.42
Net Run
Time,
minutes
48.25
48.50
48.75
49.00
49.25
49.50
49.75
50.00
50.25
50.50
50.75
51.00
51.25
51.50
51.75
52.00
52.25
52.50
52.75
53.00
53.25
53.50
53.75
54.00
54.25
54.50
54.75
55.00
55.25
55.50
55.75
56.00
56.25
56.50
56.75
57.00
57.25
57.50
57.75
58.00
58.25
58.50
58.75
59.00
59.25
59.50
59.75
60.00
six-minute
rolling averages
percent opacity,
0.42
0.42
0.21
0.21
0.21
0.21
0.22
0.23
0.23
0.23
0.23
0.23
0.23
0.45
0.23
0.23
0.45
0.45
0.45
0.45
0.45
0.68
0.91
0.91
1.36
1.36
1.36
1.36
1.36
1.36
1.30
1.25
1.25
1.25
NA*
NA*
NA*
NA*
NA*
NA*
NA*
NA*
NA*
NA*
NA*
NA*
NA*
NA*
r»AUTY DURING RUN = o.98
HIGHEST SIX-MINUTE ROLLING AVERAGE =   2.08
* Due to fugitive emission obstructions, a number of readings could not be made. Running averages included the time
 lapses so that the net run time was shortened. NA indicates that for the time period, an average is Not Applicable.

-------
                        Date:
                   Start Time:
                   Stop Time:
8/29/97
 1033
 1133
   Baghouse Outlet
Run Number: O-M9-3C
Net Run
Time,
minutes
0.2S
0.50
0.75
1.00
1.25
1.50
1.75
2.00
2.25
2.50
2.75
3.00
3.25
3.50
3.75
4.00
4.25
4.50
4.75
5.00
5.25
5.50
575
6.00
6.25
6.50
6.75
7.00
7.25
7.50
7.75
8.00
8.25
8.50
8.75
9.00
9.25
9.50
9.75
10.00
10.25
10.50
10.75
11.00
11.25
11.50
11.75
12.00
six-minute
rolling averages
percent opacity,
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
0.63
0.42
0.42
0.63
0.63
0.63
0.63
0.83
1.04
1.25
1.04
1.25
1.25
1.46
1.46
1.46
1.46
1.46
1.67
1.67
1.67
1.67
1.88
1.74
1.82
Net Run
Time,
minutes
12.25
12.50
12.75
13.00
13.25
13.50
13.75
14.00
14.25
14.50
14.75
15.00
15.25
15.50
15.75
16.00
16.25
16.50
16.75
17.00
17.25
17.50
17.75
18.00
18.25
18.50
1875
19.00
19.25
19.50
19.75
20.00
20.25
20.50
20.75
21.00
21.25
21.50
21.75
22.00
22.25
22.50
22.75
23.00
23.25
23.50
23.75
24.00
six-minute
rolling averages
percent opacity,
.82
.82
.59
.59
.59
.59
.36
.14
0.91
0.91
0.68
0.68
0.68
0.68
1.14
1.14
1.14
0.91
0.91
0.95
1.00
0.75
0.95
0.91
0.91
0.91
0.91
0.91
0.91
1.36
1.36
1.36
1.36
1.59
1.59
1.59
1.36
1.36
0.91
0.91
0.91
0.91
0.91
0.87
0.83
0.87
0.65
0.65
Net Run
Time,
minutes
24.25
24.50
24.75
25.00
25.25
25.50
25.75
26.00
26.25
26.50
26.75
27.00
27.25
27.50
27.75
28.00
28.25
28.50
28.75
29.00
29.25
29.50
29.75
30.00
30.25
30.50
30:75
31.00
31.25
31.50
31.75
32.00
32.25
32.50
32.75
33.00
33.25
33.50
33.75
34.00
34.25
34.50
34.75
35.00
35.25
35.50
35.75
36.00
six-minute
rolling averages
percent opacity,
0.65
0.65
0.65
0.65
0.65
0.22
0.22
0.22
0.43
0.22
0.22
0.22
0.22
0.22
0.22
0.43
0.43
0.43
0.43
0.43
0.65
0.63
0.63
0.63
0.63
0.63
0.63
0.63
0.63
0.63
0.63
0.63
0.42
0.42
0.42
0.63
0.63
0.83
0.83
0.63
0.63
0.63
0.63
0.65
0.43
0.43
0.43
0.43
HIGHEST SIX-MINUTE BLOCK AVERAGE = 1 .82 AVE
Net Run
Time,
minutes
36.25
36.50
36.75
37.00
37.25
37.50
37.75
38.00
38.25
38.50
38.75
39.00
39.25
39.50
39.75
40.00
40.25
40.50
40.75
41.00
41.25
41.50
41.75
42.00
42.25
42.50
42.75
43.00
43.25
43.50
43.75
44.00
44.25
44.50
44.75
45.00
45.25
45.50
45.75
46.00
46.25
46.50
46.75
47.00
47.25
47.50
47.75
48.00
six-minute
rolling averages
percent opacity,
0.43
0.43
0.43
0.43
0.43
0.43
0.43
0.43
0.43
0.43
0.43
0.22
0.22
0.22
0.22
0.22
0.22
0.65
0.65
0.63
0.63
0.63
0.63
0.63
0.63
0.83
0.83
0.83
0.83 '
0.83
0.83
0.83
0.83
0.83
0.83
0.83
0.83
0.63
0.63
0.63
0.83
0.42
0.42
0.42
0.43
0.43
0.43
0.43
Net Run
Time,
minutes
48.25
48.50
48.75
49.00
49.25
49.50
49.75
50.00
50.25
50.50
50.75
51.00
51.25
51.50
51.75
52.00
52.25
52.50
52.75
53.00
53.25
53.50
53.75
54.00
54.25
54.50
54.75
55.00
55.25
55.50
55.75
56.00
56.25
56.50
56.75
57.00
57.25
57.50
57.75
58.00
58.25
58.50
58.75
59.00
59.25
59.50
59.75
60.00
six-minute
rolling averages
percent opacity,
0.43
0.22
0.22
0.43
0.43
0.65
0.65
0.65
0.68
0.68
0.68
1.14
1.14
1.14
1.14
1.14
0.91
0.91
0.91
091
0.87
0.87
1.09
1.09
1.09
1.09
1.09
0.87
0.87
0.65
0.65
0.65
0.63
0.63
0.63
0.21
0.21
0.21
0.21
0.21
0.42
0.42
0.42
0.42
0.63
0.63
0.42
NA*
RAGE OPACITY DURING RUN = 0.75
HIGHEST SIX-MINUTE ROLLING AVERAGE =   1.88
* Due to fugitive emission obstructions, a number of readings
 lapses so that the net run time was shortened.  NA indicates
                   could not be made. Running averages included the time
                  that for the time period, an average is Not Applicable.

-------
                         Date:     8/29/97
                    Start Time:      1143
                    Stop Time:      1243
   Baghouse Outlet
Run Number: O-M9-3D
Net Run
Time,
minutes
0.25
0.50
0.75
1.00
1.25
1.50
1.75
2.00
2.25
2.50
2.75
3.00
3.25
3.50
3.75
4.00
4.25
4.50
475
5.00
5.25
5.50
5.75
6.00
6.25
6.50
6.75
7.00
7.25
7.50
7.75
8.00
8.25
8.50
8.75
9.00
9.25
950
9.75
10.00
10.25
10.50
10.75
11.00
11.25
11.50
11.75
12.00
HIGI-
six-minute
rolling averages
percent opacity,
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
0.50
0.50
0.50
0.48
0.48
0.24
0.24
0.23
0.23
0.43
0.42
0.43
0.45
0.45
0.45
0.45
0.45
0.45
0.45
0.23
0.23
0.23
0.23
0.23
0.23
Net Run
Time,
minutes
12.25
12.50
12.75
13.00
13.25
13.50
13.75
14.00
14.25
14.50
14.75
15.00
15.25
15.50
15.75
16.00
16.25
16.50
16.75
17.00
17.25
17.50
17.75
18.00
1825
18.50
18.75
19.00
1925
19.50
19.75
20.00
20.25
20.50
20.75
21.00
21.25
21.50
21.75
22.00
22.25
22.50
22.75
23.00
23.25
23.50
23.75
24.00
six-minute
rolling averages
percent opacity,
0.23
0.23
0.23
0.23
0.23
0.23
0.23
0.23
0.00
0.00
0.00
0.00
0.00
0.00
0.00
0.00
0.21
0.21
0.42
0.42
0.42
0.42
0.42
0.42
0.63
0.63
0.63
0.63
0.63
0.65
0.65
0.65
0.87
0.91
0.91
0.91
0.91
0.91
0.95
1.43
1.43
1.43
.19
.19
.19
.19
.19
.19
Net Run
Time,
minutes
24.25
24.50
24.75
25.00
25.25
25.50
25.75
26.00
26.25
26.50
26.75
27.00
27.25
27.50
27.75
28.00
28.25
28.50
28.75
29.00
29.25
29.50
29.75
30.00
30.25
30.50
30.75
31.00
31.25
31.50
31.75
32.00
32.25
32.50
32.75
33.00
33.25
33.50
33.75
34.00
34.25
34.50
34.75
35.00
35.25
35.50
35.75
36.00
six-minute
rolling averages
percent opacity,
.19
.19
.19
.19
.19
.14
.14
1.14
0.91
0.87
0.87
0.87
0.87
0.87
0.83
0.42
0.21
0.21
0.21
0.21
0.21
0.22
0.22
0.22
0.00
0.00
0.00
0.00
0.45
0.68
0.68
0.68
0.68
0.68
0.68
0.68
1.14
1.14
1.14
1.14
1.14
1.14
1.14
1.14
1.14
1.09
1.09
1.09
IEST SIX-MINUTE BLOCK AVERAGE = 2.08 AVE
Net Run
Time,
minutes
36.25
36.50
36.75
37.00
37.25
37.50
37.75
38.00
38.25
38.50
38.75
39.00
39.25
39.50
39.75
40.00
40.25
40.50
40.75
41.00
41.25
41.50
41.75
42.00
42.25
42.50
42.75
43.00
43.25
43.50
43.75
44.00
44.25
44.50
44.75
45.00
45.25
45.50
45.75
46.00
46.25
46.50
46.75
47.00
47.25
47.50
47.75
48.00
RAGEO
six-minute
rolling averages
percent opacity,
1.09
1.09
1.30
1.30
0.91
0.71
0.71
0.75
0.79
0.79
' 0.79
0.79
0.28
0.28
0.56
0.56
0.56
0.56
1.11
l.ll
1.11
1.39
1.39
1.67
1.67
1.94
2.22
2.11
2.00
1.90
2.14
2.05
2.17
2.17
2.17
2.61
2.50
2.92
2.71
2.71
2.71
2.92
2.50
2.50
2.50
2.29
2.29
2.08
Net Run
Time,
minutes
48.25
48.50
48.75
49.00
49.25
49.50
49.75
50.00
50.25
50.50
50.75
51.00
51.25
51.50
51.75
52.00
52.25
52.50
52.75
53.00
53.25
53.50
53.75
54.00
54.25
54.50
54.75
55.00
55.25
55.50
55.75
56.00
56.25
56.50
56.75
57.00
57.25
57.50
57.75
58.00
58.25
58.50
58.75
59.00
59.25
59.50
59.75
60.00
^AcTl'Y DURING RUN =
six-minute
rolling averages
percent opacity,
2.29
2.08
.88
.88
.88
.88
.67
.67
.46
.88
.88
.46
.46
.04
.04
1.04
1.04
0.83
0.83
0.83
0.83
0.83
0.83
0.83
0.63
0.63
0.42
0.42
0.42
0.42
0.42
0.42
0.42
0.00
0.00
0.00
0.00
0.00
0.00
0.00
0.00
0.00
0.00
0.00
0.00
0.00
0.00
0.00
0.81
HIGHEST SIX-MINUTE ROLLING AVERAGE =   2.92
* Due to fugitive emission obstructions, a number of readings could not be made.  Running averages included the time
  lapses so that the net run time was shortened. NA indicates that for the time period, an average is Not Applicable.

-------
Summary of Stack Gas Parameters and Test Results
/hrrtHtr 7*ftorr"8" - Gary, North Carolina
US EPA Test Method 23 - PCDD / PCDF
Baghouse Outlet
Page 1 of 6




Y
AH
Pbar
vm
Tm
"static
Ts
Vlc
CO2
02
N2
CP
AP1"
0
Dn

An
Vm(std)
Vm(std)
PS
Bws
vwstd
1-BWS
Md
Ms
vs
A
Qa
Q,
Qs(cmm)
I
RUN NUMBER
RUN DATE
RUN TIME
MEASURED DATA
Meter Box Correction Factor
Avg Meter Orifice Pressure, in. H2O
Barometric Pressure, inches Hg
Sample Volume, ft3
Average Meter Temperature, °F
Stack Static Pressure, inches H20
Average Stack Temperature, °F
Condensate Collected, ml
Carbon Dioxide content, % by volume
Oxygen content, % by volume
Nitrogen content, % by volume
Pilot Tube Coefficient
Average Square Root Dp, (in. H2O)1/2
Sample Run Duration, minutes
Nozzle Diameter, inches
CALCULATED DATA
Nozzle Area, ft2
Standard Meter Volume, dscf
Standard Meter Volume, dscm
Stack Pressure, inches Hg
Moisture, % by volume
Standard Water Vapor Volume, ft3
Dry Mole Fraction
Molecular Weight (d.b.), Ib/lb-mole
Molecular Weight (w.b.), Ib/lb-mole
Stack Gas Velocity, ft/s
Stack Area, ft2
Stack Gas Volumetric flow, acfm
Stack Gas Volumetric flow, dscfm
Stack Gas Volumetric flow, dscmm
Isokinetic Sampling Ratio, %
R-M23-0-1
8/27/97
0940-1516

0.982
3.04
29.80
226.829
111
-1.5
283
2083.3
4.0
15.0
81.0
0.84
1 .0260
240
0.256

0.000357
206.781
5.855
29.69
32.2
98.061
0.678
29.24
25.62
72.8
11.23
49,075
23,450
664.0
115.5
R-M23-0-2
8/28/97
0746-1229

0.982
2.69
29.60
208.171
97
-1.4
287
1620.9
4.9
13.6
81.5
0.84
1.0561
240
0.256

0.000357
192.849
5.461
29.50
28.3
76.296
0.717
29.33
26.12
74.7
11.23
50,303
25,122
711.4
100.5
R-M23-O-3
8/29/97
0809-1236

0.982
2.86
29.60
226.098
98
-1.3
268
1087.4
3.0
16.3
80.7
0.84
1.0760
240
0.251

0.000344
209.298
5.927
29.50
19.6
51.184
0.804
29.13
26.94
74.0
11.23
49,832
28,612
810.2
99.6
Average of
1st and 2nd
Test Run

0.982
2.87
29.70
217.5
103.8
-1.45
285.0
1852.1
4.45
14.3
81.25
0.84
1.0410
240.0
0.256

0.000357
199.815
5.658
29.59
30.3
87.178
0.697
29.28
25.87
73.7
11.23
49,689
24,286
687.7
108.0

-------
Summary of Stack Gas Parameters and Test Results
fapwitrPiwrVp" - Gary, North Carolina
US EPA Test Method 23 - PCDD / PCDF
Baghouse Outlet
Page 2 of 6






(ng)
(ng/dscm)
(pg/hr)

(ng)
(ng/dscm)
(pg/hr)

(ng)
(ng/dscm)
(pg/hr)

(ng)
(ng/dscm)
(pg/hr)

(ng)
(ng/dscm)
(pg/hr)

(ng)
(ng/dscm)
(pg/hr)
RUN NUMBER
RUN DATE
RUN TIME
EMISSIONS DATA
DIOXINS:
2378 TCDD
Catch, ng
Concentration, ng/dscm, as measured
Emission Rate, pg/hr
Total TCDD
Catch, ng
Concentration, ng/dscm, as measured
Emission Rate, pg/hr
12378 PeCDD
Catch, ng
Concentration, ng/dscm, as measured
Emission Rate, pg/hr
Total PeCDD
Catch, ng
Concentration, ng/dscm, as measured
Emission Rate, pg/hr
123478 HxCDD
Catch, ng
Concentration, ng/dscm, as measured
Emission Rate, pg/hr
123678 HxCDD
Catch, ng
Concentration, ng/dscm, as measured
Emission Rate, pg/hr
R-M23-O-1
8/27/97
0940-1516



ND
ND
ND

ND
ND
ND

ND
ND
ND

{0.530}
{0.0905}
{3.61}

ND
ND
ND

ND
ND
ND
R-M23-0-2
8/28/97
0746-1229



ND -
ND
ND

ND
ND
ND

ND
ND
ND

{1.00}
{0.183}
{7.82}

ND
ND
ND

ND
ND
ND
R-M23-0-3
8/29/97
0809-1236



ND
ND
ND

ND
ND
ND

ND
ND
ND

ND
ND
ND

ND
ND
ND

ND
ND
ND
Average of
1st and 2nd
Test Run



ND
ND
ND

ND
ND
ND

ND
ND
ND

{0.765}
{0.137}
{5.71}

ND
ND
ND

ND
ND
ND
()  Not Detected.  Value shown is the detection limit for that sample.
{}  Estimated Maximum Possible Concentration.

-------
Summary of Stack Gas Parameters and Test Results
/fspwfer ft/fc^'fc" - Gary, North Carolina
US EPA Test Method 23 - PCOD / PCDF
Baghouse Outlet
Page 3 of 6






(ng)
(ng/dscm)
(pg/hr)

(ng)
(ng/dscm)
(pg/hr)

(ng)
(ng/dscm)
(Mfl/hr)

(ng)
(ng/dscm)
(pg/hr)

(ng)
(ng/dscm)
(pg/hr)

(ng)
(ng/dscm)
(pg/hr)
RUN NUMBER
RUN DATE
RUN TIME
EMISSIONS DATA -Continued
DIOXINS - Continued
123789 HxCDD
Catch, ng
Concentration, ng/dscm, as measured
Emission Rate, pg/hr
Total HxCDD
Catch, ng
Concentration, ng/dscm, as measured
Emission Rate, pg/hr
1234678 HpCDD
Catch, ng
Concentration, ng/dscm, as measured
Emission Rate, pg/hr
Total HpCDD
Catch, ng
Concentration, ng/dscm, as measured
Emission Rate, pg/hr
1 2346789 OCDD
Catch, ng
Concentration, ng/dscm, as measured
Emission Rate, pg/hr
Total PCDD
Catch, ng
Concentration, ng/dscm, as measured
Emission Rate, pg/hr
R-M23-O-1
8/27/97
0940-1516



ND
ND
ND

ND
ND
ND

ND
ND
ND

ND
ND
ND

ND
ND
ND

{0.530}
{0.0905}
{3.61}
R-M23-O-2
8/28/97
0746-1229



ND -
ND
ND

0.440
0.0806
3.44

ND
ND
ND

{1.00}
{0.183}
{7.82}

ND
ND
ND

{2.44}
{0.447}
{19.1}
R-M23-O-3
8/29/97
0809-1236



ND
ND
ND

ND
ND
ND

ND
ND
ND

ND
ND
ND

ND
ND
ND

0.00
0.00
0.00
Average of
1st and 2nd
Test Run



ND
ND
ND

0.220
0.040
1.720

ND
ND
ND

{0.500}
{0.0916}
{3.91}

ND
ND
ND

{1.49}
{0.269}
{11-3}
()   Not Detected.  Value shown is the detection limit for that sample.
{}   Estimated Maximum Possible Concentration.

-------
Summary of Stack Gas Parameters and Test Results
/krfMw-KjMT "8" - Gary, North Carolina
US EPA Test Method 23 - PCDD / PCDF
Baghouse Outlet
Page 4 of 6






(ng)
(ng/dscm)
(ug/hr)

(ng)
(ng/dscm)
(pg/hr)

(ng)
(ng/dscm)
(pg/hr)

(ng)
(ng/dscm)
(pg/hr)

(ng)
(ng/dscm)
(pg/hr)

(ng)
(ng/dscm)
(pg/hr)
RUN NUMBER
RUN DATE
RUN TIME
EMISSIONS DATA- Continued
FURANS
2378 TCDF
Catch, ng
Concentration, ng/dscm, as measured
Emission Rate, pg/hr
Total TCDF
Catch, ng
Concentration, ng/dscm, as measured
Emission Rate, pg/hr
12378 PeCDF
Catch, ng
Concentration, ng/dscm, as measured
Emission Rate, pg/hr
23478 PeCDF
Catch, ng
Concentration, ng/dscm, as measured
Emission Rate, pg/hr
Total PeCDF
Catch, ng
Concentration, ng/dscm, as measured
Emission Rate, pg/hr
1 23478 HxCDF
Catch, ng
Concentration, ng/dscm, as measured
Emission Rate, pg/hr
R-M23-O-1
8/27/97
0940-1516



ND
ND
ND

0.150
0.0256
1.02

ND
ND
ND

ND
ND
ND

ND
ND
ND

ND
ND
ND
R-M23-O-2
8/28/97
0746-1229



ND .
ND
ND

ND
ND
ND

{0.240}
{0.0439}
{1.88}

ND
ND
ND

{0.410}
{0.0751}
{3.20}

ND
ND
ND
R-M23-O-3
8/29/97
0809-1236



ND
ND
ND

ND
ND
ND

ND
ND
ND

ND
ND
ND

{0.0200}
{0.00337}
{0.164}

ND
ND
ND
1
Average of
1st and 2nd
Test Run



ND
ND
ND

0.075
0.013
0.510

{0.120}
{0.0220}
{0.938}

ND
ND
ND

{0.205}
{0.0375}
{1.60}

ND
ND
ND
()  Not Detected.  Value shown is the detection limit for that sample.
{}  Estimated Maximum Possible Concentration.

-------
Summary of Stack Gas Parameters and Test Results
fkprtitcr Put** "8" - Gary, North Carolina
US EPA Test Method 23 - PCDD / PCDF
Baghouse Outlet
Page 5 of 6






(ng)
(ng/dscm)
(pg/hr)

(ng)
(ng/dscm)
(pg/hr)

(ng)
(ng/dscm)
(pg/hr)

(ng)
(ng/dscm)
(pg/hr)

(ng)
(ng/dscm)
(pg/hr)

(ng)
(ng/dscm)
(pg/hr)
RUN NUMBER
RUN DATE
RUN TIME
EMISSIONS DATA - Continued
Furans - Continued
1 23678 HxCDF
Catch, ng
Concentration, ng/dscm, as measured
Emission Rate, jjg/hr
234678 HxCDF
Catch, ng
Concentration, ng/dscm, as measured
Emission Rate, pg/hr
123789 HxCDF
Catch, ng
Concentration, ng/dscm, as measured
Emission Rate, pg/hr
Total HxCDF
Catch, ng
Concentration, ng/dscm, as measured
Emission Rate, pg/hr
1 234678 HpCDF
Catch, ng
Concentration, ng/dscm, as measured
Emission Rate, pg/hr
1234789 HpCDF
Catch, ng
Concentration, ng/dscm, as measured
Emission Rate, pg/hr
R-M23-O-1
8/27/97
0940-1516



ND
ND
ND

ND
ND
ND

ND
ND
ND

ND
ND
ND

ND
ND
ND

ND
ND
ND
R-M23-O-2
8/28/97
0746-1229



ND
ND
ND

ND
ND
ND

{0.240}
{0.0439}
{1.88}

{0.460}
{0.0842}
{3.60}

ND
ND
ND

ND
ND
ND
R-M23-O-3
8/29/97
0809-1236



ND
ND
ND

ND
ND
ND

ND
ND
ND

ND
ND
ND

ND
ND
ND

ND
ND
ND
Average of
1st and 2nd
Test Run



ND
ND
ND

ND
ND
ND

{0.120}
{0.0220}
{0.938}

{0.230}
{0.0421}
{1 .80}

ND
ND
ND

ND
ND
ND
()  Not Detected.  Value shown is the detection limit for that sample.
{}  Estimated Maximum Possible Concentration.

-------
Summary of Stack Gas Parameters and Test Results
ftspttAir 7W-"g" - Gary, North Carolina
US EPA Test Method 23 - PCDD / PCDF
Baghouse Outlet
Page 6 of 6






(ng)
(ng/dscm)
(pg/hr)

(ng)
(ng/dscm)
(Mg/hr)

(ng)
(ng/dscm)
(pg/hr)

(ng)
(ng/dscm)
(|jg/hr)
RUN NUMBER
RUN DATE
RUN TIME
EMISSIONS DATA - Continued
Furans - Continued
Total HpCDF
Catch, ng
Concentration, ng/dscm, as measured
Emission Rate, pg/hr
1 2346789 OCDF
Catch, ng
Concentration, ng/dscm, as measured
Emission Rate, pg/hr
Total PCDF
Catch, ng
Concentration, ng/dscm, as measured
Emission Rate, pg/hr
Total PCDD + PCDF
Catch, ng
Concentration, ng/dscm, as measured
Emission Rate, pg/hr
R-M23-O-1
8/27/97
0940-1516



ND
ND
ND

ND
ND
ND

0.150
0.0256
1.02

{0.680}
{0.116}
{4.63}
R-M23-O-2
8/28/97
0746-1229



{0.360}
{0.0659}
{2.81}

ND
ND
ND

{1.23}
{0.225}
{9.61}

{3.67}
{0.672}
{28.7}
R-M23-O-3
8/29/97
0809-1236



ND
ND
ND

ND
ND
ND

{0.0200}
{0.00337}
{0.164}

{0.0200}
{0.00337}
{0.164}
Average of
1st and 2nd
Test Run



{0.180}
{0.0330}
{1.41}

ND
ND
ND

{0.690}
{0.125}
{5.32}

{2.18}
{0.394}
{16.7}
()  Not Detected.  Value shown is the detection limit for that sample.
{}  Estimated Maximum Possible Concentration.

-------
PCDD/PCDF Corrected Stack Gas Concentrations and 2378 TCDD Toxic Equivalent Concentrations
                         ftsrtttii-r -PUM "8"- Gary, North Carolina
                           US EPA Test Method 23 - CDD/CDF
                                   Baghouse Outlet

RUN NUMBER
RUN DATE
RUN TIME
DIOXINS:
2378 TCDD
Total TCDD
12378PeCDD
Total PeCDD
1 23478 HxCDD
123678 HxCDD
123789 HxCDD
Total HxCDD
1 234678 HpCDD
Total HpCDD
1 2346789 OCDD
Total PCDD
FURANS:
2378 TCDF
Total TCDF
12378 PeCDF
23478 PeCDF
Total PeCDF
123478 HxCDF
1 23678 HxCDF
234678 HxCDF
123789 HxCDF
Total HxCDF
1234678 HpCDF
1234789 HpCDF
Total HpCDF
12346789 OCDF
Total PCDF
Total PCDD+PCDF
CONCENTRATION
(ng/dscm, adjusted to 7% O2)
R-M23-O-1 R-M23-O-2 R-M23-O-3
08/27/97 08/28/97 08/29/97
0940-1516 0746-1229 0809-1236

ND ND ND
ND ND ND
ND ND ND
{0.213} {0.349} ND
ND ND ND
ND ND ND
ND ND ND
ND 0.153 ND
ND ND ND
ND {0.349} ND
ND ND ND
{0.213} {0.851} 0.00

ND ND ND
0.060 ND ND
ND {0.0837} ND
ND ND ND
ND {0.143} {0.0102}
ND ND ND
ND ND ND
ND ND ND
ND {0.0837} ND
ND {0.160} ND
ND ND ND
ND ND ND
ND {0 126} ND
ND ND ND
0.0604 {0.429} {0.0102}
{0.274} {1.28} {0.0102}
Average of
Island 2nd
Test Run

ND
ND
ND
{0.281}
ND
ND
ND
0.0767
ND
{0.174}
ND
{0.532}

ND
0.0302
{0.0418}
ND
{0.0715}
ND
ND
ND
{0.0418}
{0.0802}
ND
ND
{0.0628}
ND
{0.245}
{0.777}
2378-TCDD
Toxic
Equivalent
Factor

1.000

0.500

0.100
0.100
0.100

0.010

0001


0.100

0.050
0.500

0.100
0.100
0.100
0.100

0.010
0.010

0.001


2378 TOXIC EQUIVALENCIES
(ng/dscm, adjusted to 7% O2)
R-M23-O-1 R-M23-O-2 R-M23-O-3
8/27/97 8/28/97 8/29/97
0940-1516 0746-1229 0809-1236

ND ND ND

ND ND ND

ND ND ND
ND ND ND
ND ND ND

ND ND ND

ND ND ND
ND ND ND

ND ND ND

ND {0.00418} ND
ND ND ND

ND ND ND
ND ND ND
ND ND ND
ND {0.00837} ND

ND ND ND
ND ND ND

ND ND ND
ND {0.0126} ND
ND {0.0126} ND
Average of
1st and 2i
'est Run

ND

ND

ND
ND
ND

ND

ND
ND

ND

{0.0021
ND

ND
ND
ND
{0.004

ND
NC

NC
{O.OOf
{O.OOt

-------
Summary of Stack Gas Parameters and Test Results
US EPA EMC Asphalt Concrete Emissions Testing /fsprf/hr fcfatr "8 "
US EPA Test Method 29 - Multiple Metals
Baghouse Outlet
Page 1 of 4




Y
AH
Pbar
vm
Tm
Pstatic
Ts
V,c
CO2
02
N2
cp
Ap1/2
0
Dn

An
Vm(std) cf
* m(std) cm
Qm
PS
Bws
Vwstd
1-BWS
Md
Ms
Vs
A
Qa
Qscfm
Qscmm
I
RUN NUMBER
RUN DATE
RUN TIME
MEASURED DATA
Meter Box Correction Factor
Avg Meter Orifice Pressure, in. H2O
Barometric Pressure, inches Hg
Sample Volume, ft3
Average Meter Temperature, °F
Stack Static Pressure, inches H2O
Average Stack Temperature, °F
Condensate Collected, ml
Carbon Dioxide content, % by volume
Oxygen content, % by volume
Nitrogen content, % by volume
Pitot Tube Coefficient
Average Square Root Ap, (in. H2O)1/2
Sample Run Duration, minutes
Nozzle Diameter, inches
CALCULATED DATA
Nozzle Area, ft2
Standard Meter Volume, ft3
Standard Meter Volume, m3
Average Sampling Rate, dscfm
Stack Pressure, inches Hg
Moisture, % by volume
Standard Water Vapor Volume, ft3
Dry Mole Fraction
Molecular Weight (d.b.), Ib/lb-mole
Molecular Weight (w.b.), Ib/lb-mole
Stack Gas Velocity, ft/s
Stack Area, ft2
Stack Gas Volumetric flow, acfrn
Stack Gas Volumetric flow, dscfm
Stack Gas Volumetric flow, dscmm
tsokinetic Sampling Ratio, %
R-M29-O-1
8/27/97
0940-1516

0.965
2.96
29.80
237.264
109
-0.42
289
1632.0
4.0
15.0
81.0
0.84
1.0773
240
0.252

0.000346
213.024
6.032
0.888
29.77
26.5
76.818
0.735
29.24
26.26
75.7
11.23
51,035
26,285
744
109.5
R-M29-O-2
8/28/97
0746-1229

0.965
2.14
29.60'
200.329
97
-0.4
292
1484.6
4.9
13.6
81.5
0.84
1.0386
240
0.252

0.000346
182.236
5.160
0.759
29.57
27.7
69.880
0.723
29.33
26.19
73.5
11.23
49,516
24,833
703
99.2
R-M29-O-3
8/29/97
0809-1236

0.965
2.80
29.60
227.316
100
-0.42
274
1147.1
3.0
16.3
80.7
0.84
1.0852
240
0.252

0.000346
205.914
5.831
0.858
29.57
20.8
53.994
0.792
29.13
26.82
75.0
11.23
50,521
28,440
805
97.8
Average of
1st and 2nd
Test Runs

0.965
2.55
29.70
218.797
103
-0.41
291
1558.3
4.5
14.3
81.3
0.84
1.0580
240
0.252

0.000346
197.630
5.596
0.823
29.67
27.1
73.349
0.729
29.28
26.22
74.6
11.23
50,276
25,559
724
104.3

-------
Summary of Stack Gas Parametere and Test Results
US EPA EMC Asphalt Concrete Emissions Testing - AsTrMcr PL
*urwtf"

US EPA Test Method 29 - Multiple Metals


RUN NUMBER
RUN DATE
RUN TIME
EMISSIONS DATA
Particulate Matter
g Target Catch, g
gr/dscf Concentration, gr/dscf
gr/dscf at 7% Concentration, gr/dscf at 7% O2
g/dscm Concentration, g/dscm
g/dscm at 7% Concentration, g/dscm at 7% O2
Ib/hr Emission Rate, Ib/hr
kg/hr Emission Rate, kg/hr
Antimony
pg Target Catch, pg
pg/dscm Concentration, pg/dscm
pg/dscm at 7% Concentration, pg/dscm at 7% O2
g/hr Emission Rate, g/hr
Arsenic
pg Target Catch, pg
pg/dscm Concentration, pg/dscm
pg/dscm at 7% Concentration, pg/dscm at 7% O2
g/hr Emission Rate, g/hr
Barium
pg Target Catch, pg
pg/dscm Concentration, pg/dscm
pg/dscm at 7% Concentration, pg/dscm at 7% O2
g/hr Emission Rate, g/hr
Beryllium
pg Target Catch, pg
pg/dscm Concentration, pg/dscm
pg/dscm at 7% Concentration, pg/dscm at 7% O2
g/hr Emission Rate, g/hr
Cadmium
pg Target Catch, pg
pg/dscm Concentration, pg/dscm
pg/dscm at 7% Concentration, pg/dscm at 7% O2
g/hr Emission Rate, g/hr
Baghouse Outlet
Page 2 of 4
R-M29-O-1
8/27/97
0940-1516


0.1148
0.00832
0.0196
0.0190
0.0448
1.87
0.850

3.84
0.637
1.50
0.0284

ND
ND
ND
ND

54.9
9.10
21.4
0.406

ND
ND
ND
ND

0.479
0.0794
0.187
0.00355


R-M29-0-2
8/28/97
0746-1229


0.0982
0.00832
0.01 58
0.0190
0.0362
1.77
0.803

3.58
0.693
1.32
0.0292

ND
ND
ND
ND

40.9
7.92
15.1
0.334

ND
ND
ND
ND

0.366
0.0708
0.135
0.00299




R-M29-0-3 Average of
8/29/97 1st and 2nd
0809-1236 Test


0.1766
0.01324
0.0400
0.0303
0.0915
3.23
1.463

3.91
0.671
2.03
0.0324

ND
ND
ND
ND

69.9
12.0
36.2
0.579

ND
ND
ND
ND

0.196
0.0336
0.102
0.00162
Runs


0.1065
0.0083
0.0177
0.0190
0.0405
1.82
0.8264

3.71
0.665
1.41
0.0288

ND
ND
ND
ND

47.9
8.51
18.3
0.370

ND
ND
ND
ND

0.422
0.0751
0.161
0.00327

-------
Summary of Stack Gas Parameters and Test Results
US EPA EMC Asphalt Concrete Emissions Testing • /Jsp/Mtr Tutor " £ "
US EPA Test Method 29 - Multiple Metals
Baghouse Outlet
Page 3 of 4





pg
pg/dscm
pg/dscm at 7%
g/hr

M9
pg/dscm
Mg/dscm at 7%
g/hr

P9
pg/dscm
pg/dscm at 7%
g/hr

M9
pg/dscm
pg/dscm at 7%
g/hr

Mg
pg/dscm
pg/dscm at 7%
g/hr

pg
pg/dscm
pg/dscm at 7%
g/hr
RUN NUMBER
RUN DATE
RUN TIME
EMISSIONS DATA - Continued
Chromium
Target Catch, pg
Concentration, pg/dscm
Concentration, pg/dscm at 7% 02
Emission Rate, g/hr
Colbalt
Target Catch, pg
Concentration, pg/dscm
Concentration, pg/dscm at 7% O2
Emission Rate, g/hr
Copper
Target Catch, pg
Concentration, pg/dscm
Concentration, pg/dscm at 7% O2
Emission Rate, g/hr
Lead
Target Catch, pg
Concentration, pg/dscm
Concentration, pg/dscm at 7% O2
Emission Rate, g/hr
Manganese
Target Catch, pg
Concentration, pg/dscm
Concentration, pg/dscm at 7% O2
Emission Rate, g/hr
Mercury
Target Catch, pg
Concentration, pg/dscm
Concentration, pg/dscm at 7% O2
Emission Rate, g/hr
R-M29-O-1
«/27/97
0940-1516


13.2
2.19
5.16
0.0978

ND
ND
ND
ND

9.29
1.54
3.63
0.0688

8.54
1.42
3.34
0.0632

70.0
11.6
27.4
0.519

ND
ND
ND
ND
R-M29-O-2
8/28/97
0746-1229


11.0
2.14
4.0J
0.0901

ND
ND
ND
ND

7.14
1.38
2.63
0.0584

5.30
1.03
1.95
0.0433

74.8
14.5
27.6
0.612

ND
ND
ND
ND
R-M29-O-3
8/29/97
0809-1236


12.6
2.16
6.53
0.104

ND
ND
ND
ND

15.0
2.57
7.77
0.124

6.09
1.04
3.16
0.0505

116.3
19.9
60.3
0.964

ND
ND
ND
ND
Average of
1st and 2nd
Test Runs


12.1
2.16
4.61
0.0939

ND
ND
ND
ND

8.2
1.46
3.13
0.0636

6.92
1.22
2.64
0.0533

72.4
13.1
27.5
0.565

ND
ND
ND
ND

-------
Summary of Stack Gas Parameters and Test Results
US EPA EMC Asphalt Concrete Emissions Testing • '4$l&Atf~ J*^*r
US EPA Test Method 29 • Multiple Metals
Baghouse Outlet
Page 4 of 4



pg
pg/dscm
pg/dscm at 7%
g/hr

pg
pg/dscm
pg/dscm at 7%
g/hr

pg
pg/dscm
pg/dscm at 7%
g/hr

pg
pg/dscm
pg/dscm at 7%
g/hr

pg
pg/dscm
pg/dscm at 7%
g/hr

pg
pg/dscm
pg/dscm at 7%
g/hr
RUN NUMBER
RUN DATE
RUN TIME
EMISSIONS DATA - Continued
Nickel
Target Catch, pg
Concentration, pg/dscm
Concentration, pg/dscm at 7% O2
Emission Rate, g/hr
Phosphorus
Target Catch, pg
Concentration, pg/dscm
Concentration, pg/dscm at 7% O2
Emission Rate, g/hr
Silver
Target Catch, pg
Concentration, pg/dscm
Concentration, pg/dscm at 7% O2
Emission Rate, g/hr
Selenium
Target Catch, pg
Concentration, pg/dscm
Concentration, pg/dscm at 7% O2
Emission Rate, g/hr
Thallium
Target Catch, pg
Concentration, pg/dscm
Concentration, pg/dscm at 7% O2
Emission Rate, g/hr
Zinc
Target Catch, pg
Concentration, pg/dscm
Concentration, pg/dscm at 7% O2
Emission Rate, g/hr
r "g"

R-M29-O-1 R-M29-O-2 R-M29-O-3 Avenge of
a/27/97 8/28/97 8/29/97 1st and 2nd
0940-1516 0746-1229 0809-1236 Test Runs


9.37
1.55
3.66
0.0694

110
18.2
42.9
0.814

0.378
0.0627
0.148
0.00280

5.63
0.934
2.20
0.0417

ND
ND
ND
ND

44.3
7.34
17.3
0.328


6.50
1.26
2.43
0.0531

115
22.2
42.3
0.937

0.217
0.0421
0.080
0.00177

4.58
0.888
1.69
0.0375

ND
ND
ND
ND

25.9
5.01
9.54
0.211


8.13
1.39
4.21
0.0674

145
24.9
75.2
1.20

ND
ND
ND
ND

4.91
0.843
2.55
0.0407

ND
ND
ND
ND

32.8
5.63
17.0
0.272


7.93
1.41
3.03
0.0612

112
20.2
42.6
0.876

0.298
0.0524
0.114
0.00229

2.29
0.911
1.95
0.0396

ND
ND
ND
ND

35.1
6.18
13.4
0.270

-------
         APPENDIX E




QA/QC DATA AND CERTIFICATIONS

-------

-------
                                 \
              TEMPERATURE SENSOR CALIBRATION FORM
Temperature Sensor No.
Ambient Temp. °F	37
                     -4
Reference Temp. Sensor:
Sensor Tvne V. - "\ Ic    Length 6"-
      Barometric Pressure, "Hg 7Q.*K
Date
lv/7«fc*
io|?< k>
loMto















Ref.
Point
No.
1
2
3
1
2
3
1
2
3
1
2
3
1
2
3
1
2
3
Temp.
Source
1C* UxJLr
ftJ». Gvr
to vJU.















Temp. °F
Ref.
Sensor
(V*)-?>-l
(&i) ^
^ 7 10















Test
Sensor
CW 36
c<^) ^r
((rffi^ Zc^















Temp.
Diff. %
C.20
-O.^p
o.\r .















Within
Limits
Y/N
. V
V
V















Calibrated
By
Ml*
VhOfl\
VAOVK

*







*





Temp. Diff
              (Jtef '  Temp + 40)  " ( Test
                                                    460)
                            ,
                            (Ref. Temp. + 460)
                                                          x 100 S 1  5 \

-------
              TEMPERATURE SENSOR CALIBRATION FORM
Temperature Sensor No.  fe-T-U

Ambient Temp. °F
Reference Temp. Sensor:
                               Sensor Type fc "\ Ic     Length 6

                              	   Barometric Pressure, "Hg V{ .c»6
Date
iota ta
lo/?^
Ic.^(=t1-















Ref.
Point
No.
1
2
3
1
2
3
1
2
3
1
2
3
1
2
3
1
2
3
Temp.
Source
tf Uc-W
a«J»- &«.''
Vxxl-s «J*















Temp. °F
Ref.
Sensor
3u
•^•2-
?u















Test
Sensor
3?
^
7(0




•










Temp.
Diff. %


















Whhin
Limits
Y/N


















Calibrated
By


















% Temp. Diff
     *
                 (gaf '
                                .  Temp.  + 460)
                                                           10°

-------
V
                     TEMPERATURE SENSOR CALIBRATION FORM
       Temperature Sensor No.
       Ambient Temp. °F
       Reference Temp. Sensor:
                        tew
                              Sensor Type JL_3l£—  Length 4j
                                _  Barometric Pressure, "Hg ~~ ' ~
Date
re i\ M"»
i(h»fa
1<^?<|<1*















Ref.
Point
No.
1
2
3
1
2
3
1
2
3
1
2
3
1
2
3
1
2
3
Temp.
Source
a* uir
Ci J». 4t*y
P. (JtJU--















Temp. °F
Ref.
Sensor
4*) T2-
(£^74
b^ 7^















Test
Sensor
4^s) S3
53t)^Z
^ 2/1















Temp.
Diff . %
- G.Z-o
0.3T-
o.\^















Within
Limits
Y/N
V
y
Y















Calibrated
By
BY^f*
^^
^>«n















, Temp.  «„
                                -( rest
                                                          46o,
                                   (Ref. Temp. + 460)
                                                               „ 100 s 1-5

-------
              TEMPERATURE SENSOR CALIBRATION FORM
Temperature Sensor No.
Ambient Temp. °F
30.
Sensor Type
                                Length
                                                                 4-1
                                      Barometric Pressure, "Hg  33-
Reference Temp. Sensor:
Date
^he^n-
<* leffr
Ref.
Point
No.
1
2
s|l«H 3















1
2
3
1
2
3
1
2
3
1
2
3
1
2
3
Temp.
Source
«*\J*i
P V«*<^
>-Uit-W.















Temp. °F
Ref.
Sensor
4i
^%
240















Test
Sensor
4-1
^

-------
                                        Probe or Pitot No.
Pilot Tube Inspection
                    I.EV5I.
                    *-—X
                     o
          BULLSEYS LEVEL -
             -pi
                   8
                     U"
Thermocouple Calibration
Type of Reference Thermometer
Barometric Pressure        -, *
                                _.inHg
Date
Tube Assembly Level?
Ports Damaged?
-10°•
,^10
~,0/7
,00^
.vt
,r
-------
                                Probe or Pitot No.
G
Pitot Tube Inspection
0
i— i ^
1 	 BULISEYE LEVEL)— <^
1 ^
rral IV ? )l
B«, l^M
,_n-,.JU
i.i
~z^"pi iGli
. ~ir^v __p 7 L^s^
• -• - -^.\
~^|k^
•^ 4Q '"
1 \feJs^X
\-- — ^ 	 '

Thermocouple Calibration
Type of Reference Thermometer ^ ^tvj :« 0 /««

Date
Tube Assembly Level?
Ports Damaged?
-10-<«1<+10- ..
-10°°
o¥
l.fl/3
• ,^v
^>
,5T
•J-/
,?70
jjt+ d^"^ s&
vQ/ — $j^*~^¥f>
Date Z/H/f ?
Barometric Pressure ^^^^ ^^S ' Ambient Temperature f-07 °F

Source • Reference
Temperature
tyt ^.^ Uf
>Lvir f /c/2
1 (Ref. Temp., 'F * 460) - (1
Thermocouple Absolute Temperature
Temperature Difference1
H 1 ~. <)<;^
/O/ f<502
^^ 0
'hermocovpleTemp., "F • 460)
                            (Ref T.mn

-------
                       •                  m •
                     Inspection  Data Sheet
Company Hame:
«• MHn •«!•«• OT»M> KM m f« wwr IM  I
MU « KM MM M MM M •!&* tint IMM.  j
                                            Pre-sample
                                        Date
                                                              Post Sample
                                                          Date fO-f3-1"7
                                                 level?
                                               obstructions?
                                                 damaged?
                                              -10° < 01 < +10*
                                              -10* < a» < -HO0
                                               -5" < Bi < -H5°
                                               -5° < 82 < +5°
                                                      Y
                                                      6
                                                      A
                                              •?nC     .5-03
                                             1.05 Dt < Pa < 1.5 Dt
                                                             .        .
                                                    1.05 Dt < PD < 1.5  Ot
                                                      3/16" '< Dt * 3/8
                                                    A tan Y < 0.125"
                                                    A tan 9 < 0.03125"
                                                    Pa • Pb ± 0.063"
                                                                      OOS1H.
   Comments:
P1tot tube/probe number
                                            meets or exceeds  all  specifications
       criteria and/or applicable design features* and is  hereby  assigned a
       pi tot tube calibration factor of 0.84.
                  •
                                        Signature
                               *•             Date
  •SM 40 CfA 60. vol. *Z. No. 1*0. Mttfio* 2.  »tHfy tlM nlniBUB
  2 l«e» tttMck of tiw tntn«ocouplt MM tin «tm«« 3/4 incft
  MMritton oitMtii tin pltot tuM «•« tM noszlt «i >MM «t
  tat top of tnis M««.

-------
Date OS-Aug-87 Meter Box Number M5-4
Calibrated By B Palm Initials t?0 .
NumberofRuns 5 ^YcJ»V». 	
Meter Y 1.016

Vw.Wt
Vw.fin
Vw, total
Pb
tw
Tw+460
BRY f5A^
Previous Y 1.024
Vm. init
Vm.fln
Vm. total
Tdii
Td«
Tdol
Tdof
Td.avg
Td+460
Time, mln
Time, sec
Time Total
dH
PALIBRATIC
Y
dH©
Y tolerance from avg *
dH® tol. from avg •*
AVERAGE Y
AVERAGE dH®
RUN1
907.127
912.513
5.386
29.80
64
544
MFTPR

653.019
658.402
5.383
65
69
82
84
85
545
13
30
13.50
0.50
IN RESULTS
1.017
1.764
0.00
0.05
1.021
1.818
RUN 2
912.675
918.262
5.387
29.80
84
544

658.758
664.147
5.389
86
93
84
86
87.75
547.75
9
30
9.50
1.00
1.020
1.740
0.00
0.08

RUNS
918.094
924.06
5.366
29.60
84
544

664.577
669.948
5.371
89
97
86
87
89.75
549.75
8
0
8.00
1.50
1.022
1.861
-0.00
-0.04

RUN 4
924.597
929.999
5.402
29.80
84
544
670.486
675.901
5.415
92
100
88
88
92
552
7
0
7.00
2.00
1.023
1.869
-0.00
-0.05

RUNS
930.307
936.958
6.651
29.80
65
545
676.205
682.864
6.659
93
104
88
89
93.5
553.5
7
0
7.00
3.00
1.023
1.854
•0.00
•0.04

RUN 6
0
0
0
29.80
0
460
0
0
0
0
0
0
0
0
460
0
0
0.00
4.00
0.000
0.000
1.02
1.82

Y error (vs prior Y) ***
-0.3%
*   must be no greater than +/- 0.02
**  must be no greater than +/- 0.20
*•• must be no greater than +/- 5%

-------
Calibrated By Richard Initial* a L)ft/\
Number of Runs 3 Jw^'v I) *
_._...__ RFFFBFNPF TF3T MFTFR ........
Meter Y 1.016

Vw, Wt
Vw.fin
Vw, total
Pb
tw
Tw+460
RUN1
643.779
652.1
8.321
29.87
61
521
RUN 2
652.614
662.322
9.708
29.87
62
522
RUNS
662.945
670.381
7.436
29.87
62
522
RUN 4
0
0
0
29.87
0
460
RUNS
0
0
0
29.87
0
460
. 	 	 , nnv f\ A 
-------
                      Date                 OS-Aug-97
                      Calibrated By         B Palm
                      Number of Run*               5
                Mater Box Number   M5-9
	 REFERENCE TEST METER 	
Mater Y 1.016

Vw.tntt
Vw.fin
Vw, total
Pb
RUN1
873.304
878.349
5.045
29.80
tw 79.5
Tw+460 539.5
RUN 2
878.537
883.6
5.083
29.80
80.5
540.5
RUNS
883.95
89O.707
6.757
29.80
81
541
RUN 4
891.057
897.317
6.26
29.80
81.5
541.5
RUNS
899.221
905.513
6.292
29.80
82
542
RUN 6
0
0
0
29.80
0
480
Previous Y 0.996
Vm, Wt
Vm.fln
Vm. total
TdH
Td»
Tdol
Tdof
Td.avg
Td+460
Time, mln
Time, sac
Time Total
dH
pAI IPtO Al
Y
dH©
Y tolerence from avg *
dH@ toL from avg **
AVERAGE Y
AVERAGE dH®
717.968
723.025
5.057
79
84
78
80
80.25
540.25
12
30
12.50
O.SO
ION RESUL
1.014
1.708
0.00
0.07
1.016
1.776
723.215
728.297
5.082
82
87
81
82
83
543
9
0
9.00
1.00
T5
1.014
1.757
0.00
0.02

728.855
735.436
6.781
85
89
83
84
85.25
545.25
10
0
10.00
1.50
1.017
1.823
-0.00
•0.05

735.791
742.073
6.282
87
91
84
85
86.75
546.75
8
0
8.00
2.00
1.017
1.813
-0.00
-0.04

743.976
750.282
6.306
88
92
85
88
87.75
547.75
8
30
6.50
3.00
1.017
1.777
-0.00
-0.00

0
0
0
0
0
0
0
0
480
0
0
0.00
4.00
0.000
0.000
0.00
0.00

                       Y error (v» prior Y) *"
2.0%
c
                       *   mutt b« no greater than +/- 0.02
                       **  must ba no graatar than +/• 0.20
                       "• must ba no graatar than +/- 5%
                       Orifice:
                         front leak check
                         back laak cheek
     X
     X

-------
Date
Calibrated By
Number of Rum
REFEREM
Meter Y 1.016

Vw.Wt
Vw.fin
Vw, total
Pb
tw
Tw+460
DRY GJ
Prevtou»Y 1.016
Vm, toft
Vm.fin
Vm, total
Tdii
Tdif
Tdol
Tdof
Td.avg
Td+460
Time, min
Time, sec
Time Total
dH
CAUBRA7
Y
dH@
Y tolerence from avg *
dH® tol. from avg »*
AVERAGE Y
AVERAGE dH®
03-Sep-«7
MMILBOUR
3
CE TEST Ml
RUN1
388.4
373.864
5.404
29.77
84
544
"kS METER -
335.123
340.601
5.478
86
86
86
86
86
546
15
0
15.00
0.40
ION RESUi:
1.016
1.685
0.00
0.00
1.016
1.686
;NE

RUN 2
373.844
378.247
5.383
29.77
83.5
543.5

340.601
346
5.399
86
85
86
85
85.5
545.5
14
48
14.80
0.40
r°
1.016
1.689
0.00
-0.00

Meter Box Number
MB* ^/n

RUN 3
379.247
384.346
5.099
29.77
83
543

346
351.11
5.11
85
85
85
85
85
545
14
0
14.00
0.40
1.017
1.683
•0.00
0.00


RUN 4
0
0
0
29.77
0
460
0
0
0
0
0
0
0
0
460
0
0
0.00
2.00
0.000
0.000
1.02
1.69

M5-9
RUNS
0
0
0
29.77
0
460
0
0
0
0
0
0
0
0
460
0
0
0.00
3.00
0.000
•0.000
1.02
1.69

Y error (v» prior Y) ***
                         0.0%
*   must be no greater than +/- 0.02
••  must be no greater than +/- 0.20
*** must be no greater than +/- 5%
Orifice:
  front leak check
  back leak check
Y
Y

-------
       DRY GAS METER AND ORIFICE CALIBRATION
CONTROL BOX NO MB-10
DATE: 12MAR97

Hd CH2O)
INITIAL WTM
FINAL WTM
INITIAL DGM
FINAL DGM
TEMP. WTM (F)
TEMP. DGM (F)
TEST TIME (MIN.)
*******************
NET VOLUME WT
NET VOLUME DO
Y
H@
RUN1
0.50
744.467
757.734
653.193
667.139
73.0
81.0
32.4
***********
13.267
13.946
0.964
1.683
BAROMETRIC PRESS. 29.50 IN. HG.
PERFORMED BY : R. GEPHART
RUN 2
0.75
758.780
770.224
668.257
680.310
74.0
84.0
23.1
***********
11.444
12.053
0.965
1.721
RUN 3
1.00
770.733
782.364
680.852
693.138
74.0
86.0
20.5
**********
11.631
12.286
0.966
1.743
RUN 4
1.50
783.592
• 795.014
694.428
706.511
74.0
87.0
16.5
************
11.422
12.083
0.965
1.754
RUN 5
2.00
795.766
807.315
707.301
719.509
74.0
88.0
14.5
***********
11.549
12.208
0.966
1.763
RUN 6
4.00
809.495
822.785
721.813
735.856
74.0
89.0
12.0
:*******
13.290
14.043
0.963
1.820
AVERAGE Y -        0.965




      ACCEPTABLE Y RANGE -




AVERAGE H@ -      1.747




      ACCEPTABLE dH@ RANGE =
0.945    TO
1.547     TO
Y - (Vw x Pb x (Td + 460)) / (Vd (Pb + (dHd /13.6)) x  (Tw + 460)
 H@ = 0.0317 x Hd / (Pb (Td + 460)) x ((Tw + 460) x time) / Vw)*2
0.985
1.947

-------
 O PACIFIC  ENVIRONMENTAL SERVICES, INC.
                                                                Central Park West
                                         5001 South Miami Boulevard, P.O. Box 12077
                                     Research Triangle Park, North Carolina 27709-2077
                                                (919) 941-0333 FAX: (919) 941-0234
                            Posttest Dry Gas Meter Calibration Form (English Units)
 Pretest Calibration Factor
 System Vacuum Setting, (in Hg)
 Reference Meter Correction Factor
    Date:     8/22/97    Pbar, in Hg
  0.965
     6
  1.004
29.90   Calibrator:
GG
Meter Box No.
MB-10
AH= 1.9
Trial
1
2
3
Duration
(min)
15
15
15
Dry Gas Meter
Initial
(ft3)
168.592
181.101
191.728
Final
(ft3)
180.101
191.728
203.498
Net
(ft3)
11.509
10.627
11.77
Initial, Inlet
(°F)
90
90
90
Final, Inle
(°F)
90
90
90
Avg. Inlet
(°F)
90
90
90
Initial, Outlet
(°F)
90
90
90
Final, Outlet
(°F)
90
90
90
Avg. Outlet
(°F)
90
90
90

Trial
1
2
3
Reference Meter
Gas Volume
Initial
(ft3)
347.479
358.341
369.176
Final
(ft3)
358.341
369.176
380.031
Net
(ft3)
10.862
10.835
10.855
Meter Temperature
Initial
(°F)
80
80
80
Final
(°F)
80
80
80
Avg.
(°F)
80
80
80
Meter Box
Correction
Factor
Y
0.961
1.038
0.939
Reference
Orifice Press
AH@
(in. H2O)
2.04
2.05
•2.05
10 08227.XLS
                        Posttest
                                                               2/26/98

-------
                                                                                                fcurv v»c;
                                                                   5001 South Miami Boulevard, P.O. Box 1207
                                                              Research Triangle Park, North Carolina 27709-207
                                                                          (919) 941-0333 FAX: (919) 941-023
                        Initial Dry Gas Meter Calibration Form (English Units)
Date:
8/19/97
in Hg
30.20 Calibrator. T. McDonald
Meter Box No.
RMB-11
AH = 0.5
Trial
1
2
3
Trial
Duration
(min)
15
15
15
Dry Gas Meter
Gas Volume
Initial
(ft3)
231.840
237.828

Final
(ft3)
237.828
243.880

Net
(ft3)
5.988
6.052
0.000
Meter Temperatures
Initial, Inlet
(°F)
81
82

Final, Inlet
(°F)
81
79

Avg. Inlet
(°F)
81
80.5
#DIV/OI
Initial, Outlet
CF)
78
80

inal, Outle
(°F)
78
78

Avg. Ou
(°F)
78
79
#DIV/(

Trial
1
2
3
Reference Meter
Gas Volume
Initial
(ft3)
257.881
263.670

Final
(ft3)
263.67
269.541

Net
(ft3)
5.789
5.871
0.000
Meter Temperature
Initial
(°F)
78
76

Rnal
(°F)
79
76

Avg.
(°F)
78.5
76
#DIV/OI
Meter Box
Correction
Factor
Y
0.967
0.976
#DIV/0!
Reference
Orifice Press
AHC
(in. H2O)
1.91
1.84
#DIV/0!
AH= 1.8
Trial
1
2
3
Trial
Duration
(min)
10
10

Dry Gas Meter
Gas Volume
Initial
(ft3)
244.055
251.377

Final
(ft3)
251.377
258.770

Net
(ft3)
7.322
7.393
0.000
Meter Temperatures
Initial, Inlet
(°F)
85
84

Final, Inlet
(°F)
80
84

Avg. Inlet
(°F)
82.5
84
#DIV/0!
Initial, Outlet
(°F)
79
79

inal, Outle
(°F)
79
79

Avg. 0
(°F
7£
7£
#D\\

Trial
1
2
3
Reference Meter
Gas Volume
Initial
(ft3)
269.71
276.902

Final
(ft3)
276.902
284.146

Net
(ft3)
7.192
7.244
0.000
Meter Temperature
Initial
(°F)
76
76

Final
(°F)
76
76

Avg.
(°F)
76
76
#DIV/0!
Meter Box
Correction
Factor
Y
0.987
0.986
#DIV/0!
Reference
Orifice Press
AH0
(in. H2O)
1.96
1.93
#DIV/0!
AH = 3.0
Trial
1
2
3
Trial
Duration
(min)
10
10

Dry Gas Meter
Gas Volume
Initial
(ft3)
258.770
268.038

Final
(ft3)
268.038
277.350

Net
(ft3)
9.268
9.312
0.000
Meter Temperatures
Initial, Inlet
(°F)
88
90

Final, Inlet
(°F)
83
86

Avg. Inlet
m
85.5
88
#DIV/0!
Initial, Outlet
CF)
80
81

inal, Outle
(°F)
79
80

Avg.
('
7
8
#D
       11 08197.XLS
                                                             10/22/97

-------
    PACIFIC ENVIRONMENTAL SERVICES. INC.
                            Central Park West
      5001 South Miami Boulevard, P.O. Box 12077
  Research Triangle Park, North Carolina 27709-2077
             (919) 941-0333 FAX: (919) 941-0234
                           Posttest Dry Gas Meter Calibration Form (English Units)
Meter Box No.                       MB-11
Dry Gas Meter No.
Orifice Manometer Setting, dH (in w.c.       2.5
System Vacuum Setting, (in Hg)            2.5
Date:
Calibrated by:
Barometric Pressure, in. Hg
Pretest Calibration Factor
                   10/13/97
                      MAD
                     29.83
                     0.987

Trial
1
2
3
Trial
Duration
(min)
6.5
7.5
6
Dry Gas Meter
Gas Volume
Initial
(ft3)
56.145
61.57
67.712
Final
(ft3)
61.57
67.712
72.705
Net
(ft3)
5.425
6.142
4.993
Meter Temperatures
Initial, Inlet
(°F)
75
78
83
Final, Inle
(°F)
78
78
87
Avg. Inlet
(8F)
76.5
78
85
Initial, Outlet
(°F)
74
76
77
Final, Outlet
en
79
78
75

Avg. Outlet
CF)
75
77
76

Trial
1
2
3
Reference Meter
Gas Volume
Initial
(ft3)
45.604
51.088
57.3
Final
(ft3)
51.088
57.3
62.309
Net
(ft3)
5.484
6.212
5.009
Meter Temperature
Initial
(°F)
78
79
79
Final
(°F)
79
79
80
Avg.
(°F)
78.5
79
79.5
Meter Box
Correction
Factor
T
1.007
1.010
1.007
Reference
Orifice1 Press
Delta-H@
(in. H2O)
2.01
2.09
2.05
                                                         AVERAGE:
                                                          % Change:
     1.0080
     2.13%
2.049

-------
    PACIFIC ENVIRONMENTAL SERVICES. INC.

                           Posttest Dry Gas Meter Calibration Form (English Units)
                                                                       Central Park West
                                                  5001 South Miami Boulevard, P.O. Box 12077
                                             Research Triangle Park, North Carolina 27709-2077
                                                        (919) 941-0333 FAX: (919) 941-0234
Reference Meter Calibration Factor       1.004
System Vacuum Setting, (in Hg)             7
                                           Pretest Calibration Factor
                                                                                            0.987
Date:
8/22/97.
in Hg
29.90 Calibrator:  GG
Meter Box No.
RMB-11
AH= 1.9
Trial
1
2
3
Duration
(min)
15
15
15
Dry Gas Meter
Initial
(ft3)
993.836
1005.384
1016.948
Final
(ft3)
1005.384
1016.948
1028.471
Net
(ft3)
11.548
11.564
11.523
Initial, Inlet
(°F)
92
92
94
Final, Inle
(T)
92
92
94
Avg. Inlet
<°F)
92
92
94
Initial, Outlet
CF)
92
92
94
Final, Outlet
(°F)
92
92
94
Avg. Outlet
(°F)
92
92
94

Trial
1
2
3
Reference Meter
Gas Volume
Initial
(ft3)
409.91
420.904
431.874
Final
(ft3)
420.904
431.874
442.814
Net
(ft3)
10.994
10.97
10.94
Meter Temperature
Initial
(°F)
80
80
80
Final
CF)
80
80
80
Avg.
(°F)
80
80
80
Meter Box
Correction
Factor
y
0.973
0.969
0.973
Reference
Orifice Press
AHO
(in. H2O)
1.99
2.00
2.00
                                                                                                                  10/21/97

-------
CM

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(V

                   VISIBLE EMISSIONS
met the specifications of Fe<£rtiiffirin^^         qualified as a visible

emissions evaluator.'Majdm^'.^^^^^Wf,^^^!^ smoke did not exceed
7.5% opacity and no sing^^rror/exceed^ ^'jpactywas incurred during the
certification test conducj^fy/Eastern Teffic#faso;-i',!-\
  ^y7    r^g&-\t:--':. .^ i'-^r?t-V^:^- -\2S7158  	
  />^v~w^	7^tt^US==	  : :.-•: :* '.} r-.^^:.; ^-^i^-jfta^,
                        Progimm Manager
                                                     DalcoTIwuc

-------
        APPENDIX F




FIELD TESTING PARTICIPANTS

-------

-------
                       FIELD TESTING PARTICIPANTS
Name
Michael Toney
Mike Maret
Marc Hamilton
Tommy Thompson
Arthur Daughtery
Allen Bass
Barry Rayfield
Jay Morgan
David Goshaw
Tom McDonald
Mike Dickerson
Affiliation
USEPA, Emission Measurement Center
Pacific Environmental Services, Inc..
DEECO"
DEECO"
DEECO"
DEECO3
DEECO3
DEECO
DEECO3
Atlantic Technical Services, Inc.3
Atlantic Technical Services, Inc.3
Responsibility
Work Assignment Manager
Project Manager
Site Leader/Console Operator
Site Leader/Console Operator
Console Operator
Console Operator
Sample Recovery
Sample Recovery
Visible Emissions Observer
Console operator
Console operator
Subcontractor to Pacific Environmental Services, Inc.

-------