United States
Environmental Protection
Agency
Office of Air Quality
Planning and Standards
Research Triangle Park, NC 27711
EPA-454/R-00-025B
May 2000
AIR
&EPA
Final Report
Hot Mix Asphalt Plants
Truck Loading and Silo Filling
Manual Methods Testing
Asphalt Plant C
Los Angeles, California
Volume 2 of 8
Clean
Mr
^JLAJEZ-^:^
•'3S&*
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FINAL REPORT
HOT MIX ASPHALT PLANTS
TRUCK LOADING AND SBLO FILLING
MANUAL METHODS TESTING
ASPHALT PLANT C, LOS ANGELES, CALIFORNIA
VOLUME 2 OF 8
APPENDIX B
EPA Contract No. 68-D-98-004
Work Assignment No. 3-02
Prepared for:
Mr. Michael L. Toney (MD-19)
Work Assignment Manager
SMTG, EMC, OAQPS
U.S. Environmental Protection Agency
Research Triangle Park, NC 27711
May 2000
Submitted by
PACIFIC ENVIRONMENTAL SERVICES, INC.
5001 S. Miami Blvd., Suite 300
Post Office Box 12077
Research Triangle Park, NC 27709-2077
(919) 941-0333
FAX (919) 941-0234
U.S. Environmental Protection Agency
Region 5, Library (PL-12J)
77 West Jackson Bpulevard, 12th Floor
Chicago, IL 60604-3590
-------
DISCLAIMER
The information in this document has been funded wholly or in part by the Office of Air
Quality Planning and Standards, U.S. Environmental Protection Agency (EPA) under contract
to Pacific Environmental Services, Inc. (PES). PES performed the work presented in this
document under three EPA contracts and seven Work Assignments; EPA Contract No. 68-D-
98-004, Work Assignment Nos. 1-08,2-07, 3-02, and 3-05, EPA Contract No. 68-D-70002,
Work Assignment Nos. 0-05 and 1-07, and EPA Contract No. 68-D-70069, Work Assignment
No. 2-16. This document has been prepared by PES, reviewed following PES' internal
quality assurance procedures, and approved by PES for distribution. This document has been
subjected to the Agency's review, and has been approved by EPA for publication as an EPA
document. Mention of trade names does not constitute endorsement by the EPA or PES.
n
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TABLE OF CONTENTS
VOLUME 1 Page
1.0 INTRODUCTION 1-1
2.0 SUMMARY OF TEST RESULTS 2-1
2.1 OVERVIEW 2-1
2.2 TREATMENT OF NON-DETECTS AND ESTIMATES 2-2
2.3 TUNNEL EXHAUST DUCT 2-2
2.4 SILO EXHAUST DUCT RESULTS 2-12
2.5 PM AND MCEM DEPOSITION ESTIMATES 2-15
2.6 METEOROLOGICAL STATION RESULTS 2-15
3.0 PROCESS DESCRIPTION 3-1
3.1 COORDINATION BETWEEN TESTING AND PROCESS
OPERATIONS 3-3
3.2 PROCESS MONITORING DURING TESTING 3-3
3.3 PROCESS SAMPLES 3-4
3.4 VELOCITY OF AIR ACROSS TOP OF TRANSPORT TRUCKS
DURING LOAD-OUT 3-5
4.0 SAMPLING LOCATIONS 4-1
4.1 TUNNEL EXHAUST DUCT 4-1
4.2 SILO EXHAUST DUCT 4-1
5.0 SAMPLING AND ANALYTICAL PROCEDURES 5-1
5.1 LOCATION OF MEASUREMENT SITES AND
SAMPLE/VELOCITY TRAVERSE POINTS 5-1
5.2 DETERMINATION OF EXHAUST GAS VOLUMETRIC
FLOW RATE 5-1
5.3 DETERMINATION OF EXHAUST GAS DRY MOLECULAR
WEIGHT 5-3
5.4 DETERMINATION OF EXHAUST GAS MOISTURE CONTENT 5-3
iii
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TABLE OF CONTENTS (CONTINUED)
VOLUME 1 rCONTINUED^ Page
5.5 DETERMINATION OF PM AND MCEM 5-3
5.6 DETERMINATION OF VOHAPs 5-3
5.7 DETERMINATION OF SVOHAPs 5-7
5.8 DETERMINATION OF WIND SPEED, WIND DIRECTION,
AMBIENT TEMPERATURE, AND AMBIENT HUMIDITY 5-7
5.9 ESTIMATE OF PM AND MCEM ON THE CEILING
OF THE LOAD-OUT TUNNEL DOWNSTREAM OF SILO NO. 5 5-7
5.10 ESTIMATE OF PM AND MCEM DEPOSITION ON THE INSIDE
WALLS OF THE SILO NO. 2 EXHAUST PLENUM 5-9
5.11 ESTIMATE OF PM AND MCEM DEPOSITION ON THE INSIDE
WALLS OF THE SILO EXHAUST DUCT 5-9
5.12 ESTIMATE OF PM AND MCEM DEPOSITION ON THE INSIDE
WALLS OF THE TUNNEL EXHAUST DUCT 5-10
6.0 QUALITY ASSURANCE/QUALITY CONTROL (QA/QC) PROCEDURES
AND RESULTS 6-1
6.1 CALIBRATION AND PREPARATION OF APPARATUS 6-1
6.2 REAGENTS AND GLASSWARE PREPARATION 6-2
6.3 ON-SITE SAMPLING 6-3
6.4 SAMPLE RECOVERY 6-4
6.5 LABORATORY ANALYTICAL QA/QC PROCEDURES 6-5
6.6 QA COORDINATOR FIELD AUDIT 6-7
APPENDIX A - TEST RESULTS AND CALCULATIONS 1
A.I TED TEST RESULTS 3
A.2 SED TEST RESULTS 101
A.3 EXAMPLE CALCULATIONS 195
A.4 PARTICIPATE DEPOSITION DATA 204
A.5 CAPTURE EFFICIENCY CALCULATIONS 211
VOLUME 2
APPENDIX B - PROCESS DATA 1
B.I PRODUCTION RECORDS FOR 7/24/98 THROUGH 7/28/98 3
B.2 PRODUCT STORAGE RECORDS FOR 7/25/98 THROUGH 7/28/98 .... 9
iv
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TABLE OF CONTENTS (CONTINUED)
VOLUME 2 (CONTINUED^
APPENDDC B - PROCESS DATA (CONTINUED)
B.3 LOAD-OUT RECORDS USED IN TED EMISSION CALCULATIONS .. 19
B.4 LOAD-OUT RECORDS FOR 6/18/98 THROUGH 7/26/98 33
B.5 LOAD-OUT RECORDS FOR 7/24/98 THROUGH 7/28/98 44
B.6 SILO NO. 2 LOAD-IN RECORDS USED IN SED EMISSION
CALCULATIONS 68
B.7 ASPHALT TEMPERATURES AT LOAD-OUT 90
B.8 MASS CHANGE RESULTS FROM ASTM TESTS PERFORMED ON
ASPHALT CEMENT SAMPLES 93
B.9 VELOCITY OF AIR ACROSS TOP OF TRANSPORT TRUCKS
DURING LOAD-OUT 100
B.10 METALS ANALYSIS OF PROCESS SAMPLES 104
VOLUME 3
APPENDDC C - FIELD DATA 1
C.I TED FIELD DATA 2
C.2 SED FIELD DATA 59
C.3 METEOROLOGICAL STATION DATA 89
C.4 ON-SITE GC/MS REPORT AND DATA 118
APPENDDC D - QA/QC DATA 230
APPENDIX E - PROJECT PARTICIPANTS 280
APPENDIX F - TEST METHODS
F.I EPA METHOD 1
F.2 EPA METHOD 1A
F.3 EPA METHOD 2
F.4 EPA METHOD 4
F.5 EPA METHOD 18
F.6 EPA METHOD 315
F.7 S W-846 METHOD 0010
F.8 SW-846 METHOD 0030
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TABLE OF CONTENTS (CONCLUDED)
VOLUME 4
APPENDIX G - ANALYTICAL DATA 1
G.I PM AND MCEM DATA la
G.2 PAH/SVOHAPS CASE NARRATIVE AND PAH DATA Ik
VOLUMES
APPENDIX G - ANALYTICAL DATA (CONTINUED) 659
G.3 SVOHAPS DATA 659
VOLUME 6
APPENDIX G - ANALYTICAL DATA (CONTINUED) 1248
G.3 SVOHAPS DATA (CONCLUDED) 1248
VOLUME?
APPENDIX G - ANALYTICAL DATA (CONTINUED) la
G.4 VOHAPS DATA Ic
VOLUMES
APPENDIX G - ANALYTICAL DATA (CONCLUDED) la
G.4 VOHAPS DATA (CONCLUDED) Ic
G.5 EPA METHOD 18 REPORT AND DATA 260
VI
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LIST OF TABLES
Page
Table 1.1 Test Log Tunnel Exhaust Duct, Asphalt Plant C - California 1-4
Table 1.2 Test Log Silo Exhaust Duct, Asphalt Plant C - California 1-5
Table 2.1 Summary of Results, Production Emissions for PM, MCEM, PAH,
SVOHAP and VOHAP, Asphalt Plant C, California - July 1998 2-3
Table 2.2 Summary of Results, Average PM and MCEM Emissions,
Asphalt Plant C, California - July 1998 2-4
Table 2.3 Summary of Results, Average PAH and SVOHAP Emissions,
Asphalt Plant C, California - July 1998 2-5
Table 2.4 Summary of Results, Average VOHAP Emissions,
Asphalt Plant C, California - July 1998 2-6
Table 2.5 Summary of Results, PAHS, SVOHAPS, & VOHAPS Average
Emissions, Silo Exhaust Duct - Asphalt Plant C, California, July 1998 2-7
Table 2.6 PM and MCEM Emissions Sampling and Exhaust Gas Parameters
Normal Operations, Tunnel Exhaust Duct, Asphalt Plant C - California .. 2-16
Table 2.7 PM and MCEM Exhaust Gas Concentrations and Emission Rates, Normal
Operations, Tunnel Exhaust Duct, Asphalt Plant C - California 2-17
Table 2.8 PAHs and Semi-Volatile Organics Emissions Sampling and
Exhaust Gas Parameters, Normal Operations, Tunnel Exhaust Duct,
Asphalt Plant C - California 2-18
Table 2.9 PAHs Exhaust Gas Concentrations and Emission Rates, Normal
Operations Tunnel Exhaust Duct, Asphalt Plant C - California 2-19
Table 2.10 Semi-Volatile Organics Exhaust Gas Concentrations and Emission Rates,
Normal Operations, Tunnel Exhaust Duct, Asphalt Plant C - California .. 2-21
Table 2.11 Volatile Organics - SW-846 Method 0030 Emissions Sampling and
Exhaust Gas Parameters, Normal Operations, Tunnel Exhaust Duct,
Asphalt Plant C - California 2-30
Table 2.12 Volatile Organics - SW-846 Method 0030 Exhaust Gas Concentrations
and Emission Rates, Normal Operation, Tunnel Exhaust Duct,
Asphalt Plant C - California 2-31
Table 2.13 Volatile Organics - EPA Method 18 Emissions Sampling and
Exhaust Gas Parameters, Normal Operations, Tunnel Exhaust Duct,
Asphalt Plant C - California 2-36
Table 2.14 Volatile Organics - EPA Method 18 Exhaust Gas Concentrations
and Emission Rates, Normal Operations, Tunnel Exhaust Duct,
Asphalt Plant C - California 2-37
Table 2.15 On-Site GC/MS Volatile Organics Exhaust Gas Concentrations and
Emission Rates with Vost (SW-846 Method 0030) and EPA Method 18
Comparison, Tunnel Exhaust Duct, Asphalt Plant C - California 7/24/98 . 2-38
Table 2.16 PM and MCEM Emissions Sampling and Exhaust Gas Parameters,
Background Condition, Tunnel Exhaust Duct, Asphalt Plant C - California 2-39
vii
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LIST OF TABLES (CONTINUED)
Page
Table 2.17 PM and MCEM Exhaust Gas Concentrations and Emission Rates,
Background Condition, Tunnel Exhaust Duct, Asphalt Plant C - California 2-40
Table 2.18 PAHs and Semi-Volatile Organics Emissions Sampling and Exhaust Gas
Parameters Background Condition, Tunnel Exhaust Duct,
Asphalt Plant C - California 2-41
Table 2.19 PAHs Exhaust Gas Concentrations and Emission Rates, Background
Condition, Tunnel Exhaust Duct, Asphalt Plant C - California 2-42
Table 2.20 Semi-Volatile Organics Exhaust Gas Concentrations and Emission Rates,
Background Condition, Tunnel Exhaust Duct, Asphalt
Plant C - California 2-44
Table 2.21 Volatile Organics - SW-846 Method 0030 Emissions Sampling and
Exhaust Gas Parameters, Background Condition, Tunnel Exhaust Duct,
Asphalt Plant C - California 2-53
Table 2.22 Volatile Organics - SW-846 Method 0030 Exhaust Gas Concentrations
and Emission Rates, Background Condition, Tunnel Exhaust Duct,
Asphalt Plant C - California 2-54
Table 2.23 Volatile Organics - EPA Method 18 Emissions Sampling and Exhaust Gas
Parameters, Background Condition, Tunnel Exhaust Duct, Asphalt
Plant C - California 2-59
Table 2.24 Volatile Organics - EPA Method 18 Exhaust Gas Concentrations and
Emission Rates, Background Condition, Tunnel Exhaust Duct,
Asphalt Plant C - California 2-60
Table 2.25 Sample Log Silo Exhaust Duct, Asphalt Plant C - California 2-61
Table 2.26 PM and MCEM Emissions Sampling and Exhaust Gas Parameters,
Silo Exhaust Duct, Asphalt Plant C - California 2-62
Table 2.27 PM and MCEM Exhaust Gas Concentrations and Emission Rates,
Silo Exhaust Duct, Asphalt Plant C - California 2-63
Table 2.28 PAHs and Semi-Volatile Organics Emissions Sampling and Exhaust Gas
Parameters, Silo Exhaust Duct, Asphalt Plant C - California 2-64
Table 2.29 PAHs Exhaust Gas Concentrations and Emission Rates, Silo Exhaust Duct,
Asphalt Plant C - California 2-65
Table 2.30 Semi-Volatile Organics Exhaust Gas Concentrations and Emission Rates,
Silo Exhaust Duct, Asphalt Plant C - California 2-67
Table 2.31 Volatile Organics - SW-846 Method 0030 Emissions Sampling and
Exhaust Gas Parameters, Silo Exhaust Duct, Asphalt Plant C - California . 2-76
Table 2.32 Volatile Organics - SW-846 Method 0030 Exhaust Gas Concentrations
and Emission Rates, Silo Exhaust Duct, Asphalt Plant C - California 2-77
Table 2.33 On-Site GC/MS Volatile Organics Exhaust Gas Concentrations and
Emission Rates with Vost (SW-846 Method 0030) Comparison,
Silo Exhaust Duct, Asphalt Plant C - California 7/25/98 2-82
Vlll
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LIST OF TABLES (CONCLUDED)
Page
Table 2.34 PM and MCEM Deposition Estimates, Asphalt Plant C - California 2-83
Table 2.35 Meteorological Data Summary, Asphalt Plant C - California 2-84
Table 3.1 Load-out Data Used in TED Emission Calculations 3-6
Table 3.2 Load-in Data for Silo No. 2 Used in SED Emission Calculations 3-7
Table 3.3 Asphalt Temperatures at Load-out, Asphalt Plant C, California 3-8
Table 3.4 Mass Change of Asphalt, Asphalt Plant C, California 3-9
Table 3.5 Results of Metals Analyses of Asphalt Samples, Asphalt Plant C,
California 3-10
Table 3.6 Air Velocity Over Transport Trucks During Load-out, Asphalt Plant C,
California 3-11
Table 5.1 Summary of Sampling and Analytical Methods, Asphalt Plant C,
California 5-2
Table 6.1 Summary of Temperature Sensor Calibration Data 6-8
Table 6.2 Summary of Pilot Tube Dimensional Data 6-9
Table 6.3 Summary of Dry Gas Meter and Orifice Calibration Data 6-10
Table 6.4 Summary of EPA Method 315 and SW-846 Method 0010
Field Sampling QA/QC Data 6-11
Table 6.5 Summary of EPA Method 315 Blank Sample Catches 6-12
Table 6.6 SW-846 Method 0010 PAHs Field and Laboratory Blanks Results,
Tunnel Exhaust Duct 6-13
Table 6.7 SW-846 Method 0010 PAHs Field and Laboratory Blanks Results,
Silo Exhaust Duct 6-14
Table 6.8 SW-846 Method 0010 PAHs Surrogate Recovery Results,
Tunnel Exhaust Duct 6-15
Table 6.9 SW-846 Method 0010 Semi-Volatile Surrogate Recovery Results
Tunnel Exhaust Duct 6-16
Table 6.10 SW-846 Method 0010 PAHs Surrogate Recovery Results,
Silo Exhaust Duct 6-17
Table 6.11 SW-846 Method 0010 Semi-Volatile Surrogate Recovery Results
Silo Exhaust Duct 6-18
Table 6.12 SW-846 Method 0030 Field and Laboratory Blanks Results
Tunnel Exhaust Duct 6-19
Table 6.13 SW-846 Method 0030 Laboratory Blank Results, Silo Exhaust Duct 6-20
Table 6.14 SW-846 Method 0030 Surrogate Recovery Results
Tunnel Exhaust Duct 6-21
Table 6.15 SW-846 Method 0030 Surrogate Recovery Results
Silo Exhaust Duct 6-22
IX
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LIST OF FIGURES
Page
Figure 1.1 Project Organization - US EPA Hot Mix Asphalt Load-out Operation,
Asphalt Plant C, California 1-6
Figure 2.1 Load-out Tunnel and MET Station Location and Average Wind Direction 2-85
Figure 3.1 Process Flow Schematic, Asphalt Plant C, California 3-2
Figure 3.2 Velocity Measurement Locations and Dimensions of Transport Trucks ..3-12
Figure 4.1 Tunnel Exhaust Duct Sampling Locations, Asphalt Plant C, California .... 4-2
Figure 4.2 Tunnel Exhaust Duct Traverse Point Locations,
Asphalt Plant C, California 4-3
Figure 4.3 Silo Exhaust Duct Sampling Locations, Asphalt Plant C, California 4-4
Figure 4.4 Silo Exhaust Duct Traverse Point Locations, Asphalt Plant C, California .. 4-5
Figure 5.1 EPA Method 315 Sampling Train Schematic 5-4
Figure 5.2 SW-846 Method 0030 Sampling Train Schematic 5-6
Figure 5.3 SW-846 Method 0010 Sampling Train Schematic 5-8
Figure 5.4 Location of TED Deposition Test Plates T,, T2, and T3 5-11
GLOSSARY OF TERMS
ASTM - American Society for Testing and Materials
CEMS - Continuous Emissions Monitoring System
CTS - Calibration Transfer Standard
EMC - Emissions Measurement Center
EMAD - Emission Monitoring and Analysis Division
ESP - Electrostatic Precipitator
FID - Flame lonization Detector
FTIR - Fourier Transform Infrared Spectroscopy
HAP - Hazardous Air Pollutant
MCEM - Methylene Chloride Extractable Matter
MRI - Midwest Research Institute
PES - Pacific Environmental Services
PM - Paniculate Matter
PTE - Permanent Total Enclosure
RAP - Recycled Asphalt
RTFOT - Rolling Thin Film Oven Test
SED - Silo Exhaust Duct
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GLOSSARY OF TERMS (CONTINUED)
SMTG - Source Measurement Technology Group
SVOHAP - Semi-Volatile Organic Hazardous Air Pollutant
TED - Tunnel Emissions Duct
TFOT - Thin Film Oven Test
THC - Total Hydrocarbons
VOHAP - Volatile Organic Hazardous Air Pollutant
VOST - Volatile Organic Sampling Train
XI
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VOLUME 2
APPENDIX B
PROCESS DATA
B.I PRODUCTION RECORDS FOR 7/24/98 THROUGH 7/28/98
B.2 PRODUCT STORAGE RECORDS FOR 7/25/98 THROUGH 7/28/98
B.3 LOAD-OUT RECORDS USED IN TED EMISSION CALCULATIONS
B.4 LOAD-OUT RECORDS FOR 6/18/98 THROUGH 7/26/98
B.5 LOAD-OUT RECORDS FOR 7/24/98 THROUGH 7/28/98
B.6 SILO NO. 2 LOAD-IN RECORDS USED IN SED EMISSION
CALCULATIONS
B.7 ASPHALT TEMPERATURES AT LOAD-OUT, 7/24/98 THROUGH 7/28/98
B.8 MASS CHANGE RESULTS FROM ASTM TESTS PERFORMED ON
ASPHALT CEMENT SAMPLES
B.9 VELOCITY OF AIR ACROSS TOP OF TRANSPORT TRUCKS DURING
LOAD-OUT
B. 10 METALS ANALYSIS OF PROCESS SAMPLES
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APPENDIX B.I
PRODUCTION RECORDS FOR 7/24/98 THROUGH 7/28/98
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-------
Pacific Environmental Services
Client/Source: Asphalt Plant C Date: 7/24/98
Data Recorded By: JHL
Time
6:34 AM
7:00 AM
7:29 AM
8:00 AM
8:30 AM
9:00 AM
9:37 AM
10:07 AM
10:41 AM
11:07 AM
11:37 AM
12:07 PM
12:37 PM
1:07 PM
Natural
Gas
Rate
(ACFM)
784
841
1320
941
1040
915
878
847
974
899
945
913
920
858
Aggregate
Feed Rate
(TPH)
184.6
295.1
458.2
409.3
383.5
328.9
322
322.6
328.6
319
320.2
319.9
320.4
320.2
Recycle
(RAP)
Feed
Rate
(TPH)
80.27
0
0
0
0
0
0
0
0
0
0
0
0
0
% RAP in
mix
28.8
0
0
0
0
0
0
0
0
0
0
0
0
0
Rubber
Feed
Rate
(TPH)
0
0
0
0
0
0
0
0
0
0
0
0
0
0
Liquid
Asphalt
Feed
Rate
(TPH)
14
15.6
24.2
21.2
21
18
16.7
16.7
18
16.6
16.6
16.6
16.6
16.6
Liquid
Asphalt
Type
4000
4000
4000
4000
4000
4000
4000
4000
4000
4000
4000
4000
4000
4000
Mix Rate
(TPH)
278.9
310.7
482.4
430.5
404.5
346.9
338.7
339.3
346.6
335.5
336.8
336.5
337
336.8
Product
Code
2C
2
2
2
4
4
2
2
4
2
2
2
2
2
Liquid
Asphalt
Temp.
(F)
329
329.3
331.8
332.2
332
331.6
330.7
330.5
333.2
327.6
326.5
326.3
328.3
330.2
330.0
Burner
Pos.
(%)
12.5
16
37.3
21
27
22
15
17
19.5
17.5
17.5
17.5
17.5
17.5
Mix
Temp. (F)
340
329.7
319.2
323.7
323.3
314.9
316.1
325.4
323.5
325
329.5
331.4
331
332.7
326.1
Cyclone
Entrance
Temp. (F)
210
217
332
268
280
262
220
227
228
229
230
229
228
228
Average
Dryer
Pressure
(in Hg)
0.29
0.27
0.31
0.33
0.28
0.27
0.31
0.31
0.31
0.3
0.32
0.31
0.31
0.27
Baghouse
Exit
Temp. (F)
209
206
280
283
262
245
220
219
220
221
222
223
221
223
Baghouse
Pressure
Drop
(in Hg)
0
0
0
0
0
0
0
0
0
0
0
0
0
0
Exhaust Fans
Amperage
(amps)
fan 1 / fan 2
75/79
75/80
81/88
75/79
80/80
75/77
75/80
73/80
80/80
76/80
75/80
75/78
73/78
73/75
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Pacific Environmental Services
Client/Source: Asphalt Plant C Date: 7/25/98
Data Recorded By: JHL
Time
6:12 AM
6:30 AM
7:10 AM
7:40 AM
8:11 AM
8:41 AM
9:11 AM
9:41 AM
10:11 AM
10:41 AM
11:10 AM
11:34 AM
12:02 PM
12:40 PM
1:13 PM
1:42 PM
Natural
Gas
Rate
(ACFM)
700
0
745
834
950
927
710
710
733
741
854
Aggregate
Feed Rate
(TPH)
69
178.8
181.3
183.2
261.2
241.6
182.4
182.7
177.2
196.4
185.5
Recycle
(RAP)
Feed
Rate
(TPH)
18.9
79.8
82.7
82.7
110.7
88.9
81.7
80.9
78.6
87.2
82.1
%RAP
in mix
20.4
29.3
29.8
29.6
28.2
25.5
29.4
29.2
29.2
29.2
29.2
Rubber
Feed
Rate
(TPH)
0
0
0
0
0
0
0
0
0
0
0
Plant shut down - lack of customers
joa
1 \J\J
812
880
899
Or44
207.7
255.86
292.7
&2
82.5
112.2
113.2
34^
27.1
29.0
26.5
0
0
0
0
Liquid
Asphalt
Feed
Rate
(TPH)
4.4
13.4
13.7
13.8
20.4
18.1
13.7
13.7
13.2
14.7
13.8
OrQ3
14
19.1
21
Liquid
Asphalt
Type
4000
4000
4000
4000
4000
4000
4000
4000
4000
4000
4000
4000
4000
4000
4000
Mix Rate
(TPH)
92.7
272
277.7
279.7
392.3
348.6
277.8
277.3
269
298.3
281.4
0-63
304.2
387.1
426.9
Product
Code
4C
2
2C
2C
4C
4C
2C
2C
2C
2C
2C
2G
2C
2C
2C
Liquid
Asphalt
Temp.
(F)
319.4
321.1
321.7
321.7
325.6
326.2
324.8
325.2
325.6
327.5
328
300 a
V7I~ \J ,\J
330
331.2
332
325.7
Burner
Pos.
(%)
11
15.1
14
17.6
21.4
'19
12
11
11.6
13
10.5
2Sr4-
15
21
20
Mix
Temp.
(F)
326.6
315.7
312.1
326.1
338
336.9
324.2
317.6
323.8
327.6
307.8
216 2
336.6
329.8
324.8
324.8
Cyclone
Entrance
Temp. (F;
210
178
228
237
281
251
221
209
218
228
208
2pg
232
260
252
Dryer
Pressure
(in Hg)
0.33
1.84
0.28
0.27
0.31
0.31
0.32
0.28
0.29
0.29
0.28
Q 23
0.29
0.29
0.27
Average
Baghouse
Exit
Temp. (F)
205
191
203
213
255
242
219
209
210
219
208
434
219
242
251
Baghouse
Pressure
Drop
(in Hg)
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
Exhaust Fans
Amperage
(amps)
fan 1 / fan 2
75/75
88/92
75/78
75/80
74/79
73/79
74/75
72/76
73/75
71/74
71/73
71/74
71/72
72/75
72/75
-------
Pacific Environmental Services
Client/Source: Asphalt Plant C Date: 7/27/98
Data Recorded By: JHL
Time
6:30 AM
6:59 AM
7:36 AM
7:55 AM
8:33 AM
8:57 AM
9:27 AM
9:57 AM
10:27 AM
10:57 AM
11:27 AM
11:57 AM
12:27 PM
12:57 PM
1:27 PM
1:57 PM
2:27 PM
Natural
Gas
Rate
(ACFM)
1190
1190
978
1280
1400
1330
1530
1470
1330
1190
1430
1420
1360
1210
1300
1120
881
Aggregate
Feed Rate
(TPH)
0.9
342.8
349.4
476.9
348.4
366.84
386.3
367.8
366.2
385.6
387.1
556
366.9
356.7
356.4
457.1
374.7
Recycle
(RAP)
Feed
Rate
(TPH)
0
140.3
145.7
0
130.6
150.9
162
154.9
152.8
144.5
157.9
37.9
152.9
161.7
158.5
60
0
%RAP
in mix
0.0
27.6
28.0
0.0
25.9
27.7
28.1
28.2
28.0
25.9
27.5
6.1
28.0
29.7
29.3
11.0
0.0
Rubber
Feed
Rate
(TPH)
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
Liquid
Asphalt
Feed
Rate
(TPH)
3.6
24.6
25.6
24.6
24.8
26.8
28.4
27.1
26.9
27.5
28.2
30.6
27
26.9
26.7
26.7
19.5
Liquid
Asphalt
Type
4000
4000
4000
4000
4000
4000
4000
4000
4000
4000
4000
4000
4000
4000
4000
4000
4000
Mix Rate
(TPH)
1.36
507.7
520.7
501.5
503.8
544.6
576.6
549.8
545.9
557.5
573.2
624.4
546.9
545.2
541.5
543.3
394.2
Product
Code
2C
2C
2C
2C
2C
2C
2C
2C
2C
2C
2C
2C
2C
2C
2C
2C
2
Liquid
Asphalt
Temp.
(F)
319.3
321.9
327.6
332.9
339.9
342.5
346.3
346.5
346.9
349
348.9
352.5
352.5
360.9
358
363.4
362.5
345.4
Burner
Pos.
(%)
24.9
31.3
27
37
35.1
36
40.1
40
40
40
40
39.5
33
38.4
26.5
33.4
17.6
Mix
Temp.
(F)
316.1
324.7
325.5
307.4
325.4
329.4
317.6
337.2
338.5
331.1
324.2
309.6
307.5
318.6
313
331.6
326.5
322.6
Cyclone
Entrance
Temp. (F)
271
341
325
341
368
354
365
372
373
370
373
357
388
370
318
289
230
Dryer
Pressure
(in Hg)
0.33
0.28
0.3
0.25
0.33
0.22
0.25
0.22
0.27
0.27
0.29
0.34
0.4
0.22
0.52
0.3
0.25
Average
Baghouse
Exit
Temp. (F)
231
306
319
298
332
329
336
343
344
345
347
331
356
343
305
323
253
Baghouse
Pressure
Drop
(in Hg)
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
Exhaust Fans
Amperage
(amps)
fan 1 / fan 2
78/81
78/81
75/80
78/82
75/81
78/83
80/90
80/88
80/87
80/88
79/85
80/89
80/88
78/80
79/83
80/85
72777
-------
Pacific Environmental Services
Client/Source: Asphalt Plant C
Time
6:46 AM
7:16 AM
7:46 AM
8: 17 AM
8:46 AM
9:16 AM
9:34 AM
9:46 AM
10:1 5 AM
10:46 AM
11:16AM
11:46 AM
12:24 PM
12:46 PM
1:16 PM
1:46 PM
2:16 PM
6:14 PM
6:44 PM
6:56 PM
7:14 PM
Natural
Gas
Rate
(ACFM)
1160
1090
1090
1000
1380
1180
1160
1130
1130
1030
1160
1180
1170
1160
1060
1010
1009
1200
921
807
919
Aggregate
Feed Rate
(TPH)
234.4
258.4
240.1
277.9
317.9
315.9
297.8
399.8
281.4
299.8
299
307.1
303.5
297.3
267.1
301.8
336.3
121.5
218
218.7
217.9
Recycle
(RAP)
Feed
Rate
(TPH)
58.3
111.6
101.8
120.1
137.1
135.7
124.8
65.4
114.6
128.7
127
129.9
128.6
121.8
113.3
139.1
126.1
43.1
95.8
95.6
94.9
% RAP
in mix
18.8
28.7
28.3
28.7
28.6
28.6
28.0
13.2
27.4
28.6
28.3
28.2
28.2
27.6
28.2
29.9
25.9
24.8
29.0
28.9
28.8
Rubbe
Feed
Rate
(TPH)
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
Liquid
Asphalt
Feed
Rate
(TPH)
16.22
19.16
17.7
20.6
23.6
23.4
23.11
29.4
21.8
22.2
22.1
22.6
23.7
21.7
20.8
25
24
8.9
16.3
16.3
16.2
Date: 7/28/98
Data Recorded By: JHL
Liquid
Asphalt
Type
4000
4000
4000
4000
4000
4000
8000
8000
4000
4000
4000
4000
4000
4000
4000
4000
4000
4000
4000
4000
4000
Mix Rate
(TPH)
309.5
389.1
359.7
418.6
478.6
474.9
445.7
494.6
417.8
450.7
448.1
460
455.7
440.9
401.2
465.9
486.5
173.5
330.1
330.6
329
Produc
Code
2B
2C
2C
2C
2C
2C
4C
10
4C
2C
2C
2C
2C
2C
4C
2C
2C
2C
2C
2C
2C
Liquid
Asphalt
Temp.
(F)
339.2
347.5
347.1
348.5
352.5
354.5
356.7
286.4
296.5
358.2
356.1
254.5
354
355.1
354.3
355.1
355.7
298.2
299
298.3
298.3
331.7
Burne
Pos.
(%)
34.3
20
22
28.3
34
33
33
33.5
30
29
32.2
32.2
31
32.3
25.3
30.3
39.2
34.4
15.2
17.3
16.8
Mix
Temp.
(F)
327.5
348.1
320.4
324
335.2
335
336
336.2
341.1
329.2
346.6
346.9
341.1
345.3
364.4
357.1
343.7
307.4
321.5
322.9
320.7
335.7
Cyclone
Entrance
Temp. (F
306
277
267
319
349
347
330
292
310
316
344
345
323
349
304
327
268
350
251
259
248
Dryer
Pressure
(in Hg)
0.31
0.28
0.3
0.29
0.32
0.25
0.29
0.27
0.33
0.29
0.29
0.31
0.29
0.26
0.28
..29
0.28
0.32
0.28
0.32
0.28
Average
Baghouse
Exit
Temp. (F
281
286
247
286
315
322
355
289
285
294
318
320
302
317
297
303
334
264
247
246
237
Baghous
Pressure
Drop
(in Hg)
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0.7
0.7
0.7
Exhaust Fans
Amperage
(amps)
fan 1 / fan 2
73/80
73/79
74/80
75/80
75/80
73/80
73/80
75/80
73/72
72/78
75/78
75/78
72/75
71/75
70/72
72/75
80/85
72/80
70/71
70/73
70/71
-------
APPENDIX B.2
PRODUCT STORAGE RECORDS FOR 7/25/98 THROUGH 7/28/98
-------
-------
SILO STORAGE - Data for 7/24/98
7:00 AM
7:24 AM
7:36 AM
7:42 AM
7:54 AM
8:05 AM
8:18 AM
8:30 AM
8:46 AM
9:00 AM
9:22 AM
9:33 AM
9:49 AM
10: 07 AM
10:28 AM
10:41 AM
10:52 AM
11:09 AM
11:24 AM
11:37 AM
12:11 PM
12:37 PM
12:56 PM
1:07 PM
191.7
191.7
191.7
191.7
191.7
187.7
145.2
145.2
145.2
145.2
145.2
145.2
145.2
103
68.5
39.2
18.84
0
0
0
0
0
0
0
0.3
53.8
123.75
177.1
174.3
211.8
214.7
193.3
87.1
62.7
90
86.1
97.9
69.8
102.3
111.8
111
111
147.9
189.2
138.8
108.4
29.2
0
145.9
82.4
61.6
40.3
15.5
15.5
15.7
31.4
88.7
112.6
70.8
49.7
0.1
0.1
0.1
63.83
126.5
124.2
131.8
89.14
64.3
43
43.2
43.2
117.8
104.1
104.1
104.1
104.1
104.1
147.8
187
187
144.7
172.6
172.6
172.6
172.6
172.6
172.6
172.6
173.5
153.4
111.2
111.2
111.2
69.1
87.8
203.4
203.4
203.4
203.4
203.4
203.4
203.4
203.4
203.4
203.4
203.4
203.4
203.4
203.4
203.4
97.88
33.71
0
0
0
0
0
0
0
II
Pagel
-------
SILO STORAGE - Data for 7/24/98
7:41 AM 1/2"
3/4"
1/2"
3/4"
\0(\
Pagel
-------
SILO STORAGE - Data for 7/25/98
6:17
7:10
7:40
9:40
11:00
empty
empty
ti
it
empty
1/2"
3/4"
it
n
3/4"
1/2"
1/2"
"
empty
3/4"
3/4"
"
empty
3/4"
3/4"
11
empty
11-
Page 1
-------
SILO STORAGE - Data for 7/25/98
6:12 AM
6:30 AM
6:56 AM
7:10 AM
7:21 AM
7:31 AM
7:40 AM
7:51 AM
8:11 AM
8:24 AM
8:41 AM
8:54 AM
9:11 AM
9:25 AM
9:41 AM
10:11 AM
10:26 AM
10:42 AM
11:00 AM
11:10AM
11:29 AM
11:34 AM
11:52 AM
12:02 PM
12:40 PM
12:56 PM
1:13 PM
1:26 PM
1:42 PM
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
138.2
57.6
57.6
7
48
56.3
84.2
82.6
132.3
132.3
89.5
117.6
163.5
141.3
101.6
59.9
98
156.8
157
163.1
212.1
full
181.2
111.3
95.8
49
83.3
102.5
120.5
164.5
201
201
198.8
198.8
154.3
121.1
75.9
19.8
54.7
92.6
63.7
42.6
0
21
6
0
0
0
0
0
0
0
0
0
0
0
0
0
65.8
149.1
149.1
174.5
174.5
174.5
174.5
174.5
174.5
153.2
128.7
105.6
63.6
63.6
63.6
63.6
63.6
0
0
0
0
0
0
0
0
0
0
0
0
217.6
196.5
154.2
111.8
90.8
90.8
90.8
90.8
90.8
69.7
69.6
48.3
48.3
48.3
48.3
48.3
48.3
30.5
0
0
0
0
0
0
0
0
0
0
0
Pagel
-------
SILO STORAGE - Data for 7/27/98
1
_L
SAME SET-UP FOR THE REMAINDER OF THE DAY
Page 1
-------
SILO STORAGE - Data for 7/27/98
6:30 AM
6:59 AM
7:14 AM
7:31 AM
7:50 AM
8:09 AM
8:33 AM
8:45 AM
8:57 AM
9:06 AM
9:20 AM
9:36 AM
9:57 AM
10:14 AM
10:27 AM
10:37 AM
10:57 AM
11:16 AM
11 :33 AM
11:57 AM
12:12 PM
12:27 PM
12:57 PM
1:12 PM
1:27 PM
2:00 PM
2:27 PM
Production
198.3
198.3
198.3
198.3
198.3
198.3
198.3
198.3
198.3
198.3
198.3
198.3
190.2
190.2
190.2
190.2
190.2
190.2
190.2
144.5
123.4
102.5
34.6
34.6
34.6
34.6
34.7
24.2
155.6
101
233.9
134.5
121.4
81.4
160.9
140.1
101.6
97.1
117.1
173.8
147.5
135.1
48
136.4
138.9
141.9
88.6
80
100.3
125.8
128.5
127.2
129
115.4
ends for the day
0.2
0.2
0.2
0.5
0.5
0.8
0.8
0.8
0.8
0.8
0.8
0.8
0.8
0.8
0.8
0.8
0.8
0.8
0.8
0.8
0.8
0.8
0.8
0.8
0.8
0.8
0.8
210
19
19
19
132.8
165.1
106.4
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
200
157.5
157.5
201.3
203
203
203
185
185
185
185
185
185
185
185
108.6
14.7
14.7
14.7
14.7
14.7
14.7
14.7
14.7
14.7
0
0
Pagel
-------
SILO STORAGE - Data for 7/28/98
Same for rest of day
Page 1
-------
SILO STORAGE - Data for 7/28/98
6:46 AM
7:16 AM
7:31 AM
7:48 AM
8:03 AM
8:18 AM
8:31 AM
8:49 AM
9:00 AM
9:19 AM
9:33 AM
9:46 AM
10:15 AM
10:33 AM
10:46 AM
11:05 AM
11:16 AM
11:36 AM
11:46 AM
12:04 PM
12:24 PM
12:46 PM
1:04 PM
1:16 PM
1:30 PM
1:48 PM
2:05 PM
2:16 PM
6:14 PM
6:26 PM
6:44 PM
6:56 PM
7:14 PM
7:36 PM
202.48
202.48
202.48
202.48
202.48
202.48
202.48
181.24
181.24
161.26
140.08
167.9
152.66
171.42
147.48
122.79
98.52
73.98
28.52
44.75
128.75
132.03
55.22
5.39
57.68
140.1
94.8
70.88
115.46
115.46
115.46
115.46
115.46
115.46
Testing ends at 7:43 PM
88.9
213.51
172.67
114.44
79.42
76.44
119.64
126.34
131.94
166.38
148.38
104.04
0
74.58
130.81
111.24
186.54
181.81
186.99
180.99
14.14
114.29
165.24
174.01
83.98
16.13
53.26
89.46
11.08
36.68
38.9
57.85
124.5
148.25
204.8
204.8
204.8
183.74
183.74
141.33
120.15
98.84
56.28
32.14
32.14
48.16
198.55
207.77
178.67
157.45
136.31
115
94.04
73.37
73.37
31.04
31.04
31.04
22.94
22.94
22.94
22.94
9.2
9.2
9.2
9.2
9.2
9.2
81.3
8.42
187.66
217.53
217.53
217.53
167.46
167.46
167.46
167.46
167.46
167.46
167.46
105.65
105.65
105.65
105.65
105.65
105.65
132.21
132.21
116.7
116.7
116.7
116.7
37.15
37.15
37.15
146.84
146.84
146.84
146.84
146.84
146.84
200
174.36
174.36
201.87
201.87
201.87
201.87
201.87
201.87
201.87
201.87
201.87
85.96
85.96
85.96
85.96
34.88
9.3
9.3
9.3
9.3
9.3
9.3
9.3
9.3
9.3
9.3
9.3
198.69
156.57
156.1
156.1
156.1
156.1
11-
Page 1
-------
-------
-------
APPENDIX B.3
LOAD-OUT RECORDS USED IN TED EMISSION CALCULATIONS
-------
-------
Hot Mix Asphalt Plant C Load-Out Data
Data used in TED Emission Calculations
Client/Source
Date
7/24/98
7/24/98
7/24/98
7/24/98
7/24/98
7/24/98
7/24/98
7/25/98
7/25/98
7/25/98
7/25/98
7/25/98
7/25/98
7/25/98
7/27/98
7/27/98
7/27/98
7/27/98
7/27/98
7/27/98
7/27/98
/^/28/9fe
\ 7/28/98
A7/M798
7/2*/98
/ 7/28\98
7/28/98
V7/28/9S
EPA Plant C
Hot Mix Asphalt
Test
Method
T-V-1-1
T-V-1-2
T-V-1-3
T-V-1-4
T-MM5-1
T-M315-1
T-M18-1
T-V-2-1
T-V-2-2
T-V-2-3
T-V-2-4
T-MM5-2
T-M315-2
T-M18-2
T-V-3-1
T-V-3-2
T-V-3-3
T-V-3-4
T-MM5-3
T-M315-3
T-M18-3
T-V-4-1
T-V-4-2
T-V-4-3
T-V-4-4
T-MM5-4
T-M3154
T-M18-4
Total Tons
169.9
262.3
276.9
297.2
1832.8
1875.0
1853.8
177.8
182.6
162.9
62.8
1478.7
1499.7
1499.7
258.4
292.2
273.9
2530.2
2529.7
2530.2
Run No.
Date:
Data Collected By:
Spreadsheet work;
Summary Runs 1-4
NA
P.S. Murowchick
Derek Hawkes
no data sheet
background
background
background
background
background
background
background
# T-vJ-4- T«*t^
~,
/
final.xls
Q9IW98
-------
Hot Mix Asphalt Plant C Load-Out Data
Data used in TED Emission Calculations
Client/Source
EPA Plant C
Run No
Data:
Hot Mix Asphalt Data Collected By
Spraadthael work
Time
Of
Loading
7:13
7:15
7:17
7:19
7:28
7:32
7:38
7:41
7:43
7:45
7:46
7:48
7:49
7:52
7:56
7:58
7:59
8:02
8:05
8:07
8:12
8:15
8:23
8:24
8:27
8:28
8:30
8:33
8:38
8:39
8:41
8:43
8:46
8:49
8:50
8:52
8:54
8:55
8:59
9:03
9:05
9:10
Actual
Tons
Loaded
20.86
20.88
21.34
20.92
20.89
21.45
21.20
21.34
20.83
21.39
20.10
21.04
4.03
21.19
21.12
3.99
21.27
21.12
21.17
21.25
21.39
21.16
21.40
20.91
2.54
21.22
21.43
21.20
21.22
21.36
21.35
21.05
20.94
21.38
21.33
21.12
21.04
21.17
21.26
20.88
19.91
21.22
Silo
No.
4
3
4
4
3
2
3
2
3
2
2
,_ 2
3
2
2
1
2
2
2
1
2
1
2
3
3
2
3
2
2
2
3
2
3
2
2
4
3
4
2
3
2
2
T-V-1 (1-4)
1
1
1
1
1
1
1
1
2
1-Load Out
7/24/1998
P.S. Murowchick
Derek Hawkes
T-MM5-1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
T-M315-1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
T-M18-1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
flnal.xls
09/28/98
-------
Hot Mix Asphalt Plant C Load-Out Data
Data used in TED Emission Calculations
Client/Source
EPA Plant C
Run No.
Date.
1-Load Out
7/24/1998
Hot Mix Asphalt Data Collected By P.S. MUPOWChlck
Spreadsheet woric
Time
Of
Loading
9:12
9:16
9:21
9:22
9:24
9:28
9:33
9:37
9:38
9:39
9:42
9:44
9:45
9:49
9:50
9:53
9:55
9:58
10:00
10:02
10:05
10:06
10:07
10:09
10:11
10:14
10:27
10:28
10:30
10:33
10:35
10:36
10:38
10:40
10:41
10:43
10:46
10:52
10:56
10:58
11:00
11:01
Actual
Tons
Loaded
21.10
21.04
21.10
21.58
21.27
21.46
21.44
21.42
21.36
21.20
21.06
7.00
21.13
20.88
21.34
21.20
21.53
21.52
21.29
21.60
20.94
21.27
21.22
20.96
21.44
21.06
21.50
20.43
21.41
21.29
21.08
21.39
21.33
21.14
21.45
21.25
21.26
21.40
21.40
21.07
21.51
21.33
Silo
No.
3
4
3
2
2
2
2
3
2
2
2
3
3
2
2
3
2
2
2
2
1
2
2
1
2
2
1
5
5
1
5
5
5
1
5
5
5
1
5
3
4
5
T-V-1 (1-4)
2
2
2
2
2
2
2
2
2
2
2
2
3
3
3
Derek Hawkes
T-MM5-1
1
1
1
1
1
1
1
1
1
1
1
1
1
T-M315-1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
T-M18-1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
09/28/98
final.xls
-------
Hot Mix Asphalt Plant C Load-Out Data
Data used in TED Emission Calculations
Run NO. 1-Load Out
Client/Source
EPA Plant C
Date.
Hot Mix Asphalt Data Collected By:
Spreadsheet work
Time
Of
Loading
11:09
11:10
11:12
11:17
11:18
11:22
11:23
11:24
11:26
11:28
11:33
11:36
11:38
11:39
11:40
11:41
11:43
11:45
11:50
11:53
11:55
11:57
12:02
12:04
12:05
12:10
12:15
12:17
12:19
12:22
12:23
12:25
12:30
12:35
12:36
12:37
12:38
12:40
12:42
12:44
12:46
12:48
Actual
Tons
Loaded
21.29
21.34
21.42
21.30
21.29
21.40
21.45
20.78
21.43
21.32
21.35
21.19
21.12
21.14
24.84
21.17
20.12
21.34
21.06
21.15
21.31
21.35
21.22
21.32
21.22
21.02
23.99
21.29
21.00
21.52
21.47
21.46
21.33
20.40
21.73
21.28
21.16
21.39
20.33
21.57
Silo
No.
4
3
4
4
3
4
4
4
3
2
2
3
2
2
3
3
2
2
2
2
2
2
2
2
2
2
2
2
2
2
2
2
2
3
2
2
2
2
2
2
2
4
T-V-1 (1-4)
3
3
3
3
3
3
3
3
3
3
4
4
4
4
4
4
4
4
4
4
4
4
4
4
7/24/1998
P.S. Murowchick
Derek Hawkes
T-MM5-1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
T-M315-1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
T-M18-1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
final.xls
09/28/98
-------
Hot Mix Asphalt Plant C Load-Out Data
Data used in TED Emission Calculations
Client/Source
EPA Plant C
Run No
Date
Hot Mix Asphalt Data Collected By
Spreadsheet work.
Time
Of
Loading
12:49
12:51
12:53
12:54
12:56
13:01
13:02
Total
Actual
Tons
Loaded
21.25
21.20
21.17
21.31
21.19
2673.49
Silo
No.
4
4
2
2
2
4
T-V-1 (1-4)
4
1-Load Out
7/24/1998
P.S. Murowchick
Derek Hawkes
T-MM5-1
1
1
1
1
1832.8
T-M315-1
1
1
1
1
1
1
1875.0
T-M18-1
1
1
1
1
1853.8
final.xls
09/28/98
-------
Hot Mix Asphalt Plant C Load-Out Data
Data used in TED Emission Calculations
Client/Source-
EPA Plant C
Run No.
Date
Hot Mix Asphalt Data Collected By.
Spreadsheet work:
Time
Of
Loading
7:02
7:04
7:08
7:09
7:12
7:20
7:21
7:23
7:24
7:25
7:29
7:31
7:32
7:35
7:38
7:40
7:42
7:43
7:44
7:45
7:47
7:48
7:51
7:53
7:55
7:57
7:59
8:05
8:07
8:10
8:14
8:17
8:17
8:19
8:20
8:02
8:24
8:25
8:28
8:30
8:32
8:34
Actual
Tons
Loaded
21.12
21.43
21.24
21.02
20.92
23.87
23.65
21.21
23.93
21.09
24.43
L 20.59
23.24
20.64
24.47
!_21.26
L 24.52
21.32
21.26
19.73
21.05
21.45
21.31
24.65
24.48
21.13
24.03
21.50
21.16
21.27
21.25
Silo
No.
2
5
2
3
5
3
2
2
3
3
2
3
3
3
2
2
3
2
2
2
3
3
2
3
3
3
2
3
2
3
4
3
3
3
3
5
3
3
2
3
3
2
T-V-2 (1-4)
1
1
1
1
1
1
1
1
1
1
1
2-Load Out
7/25/1998
P.S. Murowchick
Derek Hawkes
T-MM5-2
2
2
2
2
2
2
2
2
2
2
2
2
2
L 2
2
2
2
2
2
2
2
2
2
2
2
2
2
2
2
2
2
2
2
2
2 j
2
2
2
T-M315-2
2
2
2
2
2
2
2
2
2
2
2
2
2
2
2
2
2
2
2
2
2
2
2
2
2
2
2
2
2
2
2
2
2
2
2
2
2
2
T-M18-2
2
2
2
2
2
2
2
2
2
2
2
2
2
2
2
2
2
2
2
2
2
2
2
2
2
2
2
2
2
2
2
2
2
2
2
2
2
2
fmal.xls
09/28/98
-------
Hot Mix Asphalt Plant C Load-Out Data
Data used in TED Emission Calculations
Client/Source
EPA Plant C
Run No.
Data
Hot Mix Asphalt Data CoHectad By
SpraadshMt woric
Time
Of
Loading
8:37
8:38
8:39
8:42
8:45
8:46
8:48
8:50
8:51
8:52
8:59
9:00
9:02
9:03
9:06
9:10
9:13
9:15
9:17
9:18
9:21
9:23
9:24
9:28
9:31
9:33
9:35
9:40
9:41
9:45
9:47
9:48
9:49
9:54
9:55
9:57
9:59
9:59
10:02
10:05
10:06
10:09
Actual
Tons
Loaded
24.45
21.26
21.30
23.21
21.00
24.47
21.18
23.80
21.00
20.80
21.18
23.67
20.89
20.87
21.02
12.00
21.01
24.19
20.93
20.94
8.00
21.10
23.87
15.03
24.58
21.17
23.58
20.86
22.79
20.70
24.19
21.06
Silo
No.
4
4
3
5
4
4
3
2
2
2
2
2
3
4
4
2
3
2
2
2
2
2
3
2
2
2
3
2
2
2
2
2
2
2
2
2
2
2
2
2
2
T-V-2 (1-4)
2
2
2
2
2
2
2
2
2
2
2
3
3
3
3
3
3
3
3
3
2-Load Out
7/25/1998
P.S. Murowchick
Derek Hawkes
T-MM5-2
2
2
2
2
2
2
2
2
2
2
2
2
2
2
2
2
2
2
2
2
2
2
2
2
2
2
2
2
2
2
2
2
2
2
T-M315-2
2
2
2
2
2
2
2
2
2
2
2
2
2
2
2
2
2
2
2
2
2
2
2
2
2
2
2
2
2
2
2
2
2
2
T-M18-2
2
2
2
2
2
2
2
2
2
2
2
2
2
2
2
2
2
2
2
2
2
2
2
2
2
2
2
2
2
2
2
2
2
2
fmal.xls
09/28/98
-------
Hot Mix Asphalt Plant C Load-Out Data
Data used in TED Emission Calculations
Client/Source
EPA Plant C
Run No.
Date:
Hot Mix Asphalt Data Collected By:
Spreadsheet work:
Time
Of
Loading
10:14
10:15
10:16
10:27
10:28
10:30
10:32
10:35
10:39
10:41
10:43
10:46
10:48
10:50
10:52
10:54
11:00
11:04
11:10
11:19
11:24
Total
Actual
Tons
Loaded
23.54
6.18
24.06
20.91
21.06
20.79
3.14
17.89
21.00
14.52
6.38
20.80
20.87
20.91
20.91
21.07
21.13
20.64
21.01
1707.13
Silo
No.
2
2
3
2
2
4
4
4
4
5
5
5
2
2
2
2
2
2
2
2
T-V-2 (1-4)
3
3
3
4
4
4
2-Load Out
7/25/1998
P.S. Murowchick
Derek Hawkes
T-MM5-2
2
2
2
2
2
2
2
2
2
2
2
2
2
2
2
2
2
2
2
2
1478.7
T-M315-2
2
2
2
2
2
2
2
2
2
2
2
2
2
2
2
2
2
2
2
2
2
1499.7
T-M18-2
2
2
2
2
2
2
2
2
2
2
2
2
2
2
2
2
2
2
2
2
2
1499.7
final.xls
09/28/98
-------
Hot Mix Asphalt Plant C Load-Out Data
Data used in TED Emission Calculations
Client/Source
EPA Plant C
Hot Mix Asphalt
Run No
Date:
Data Collected By:
Spreadsheet work;
Time
Of
Loading
7:02
7:04
7:09
7:11
7:13
7:18
7:36
7:37
7:38
7:39
7:43
7:44
7:46
7:47
7:53
7:54
7:55
7:56
8:00
8:01
8:02
8:03
8:04
8:09
8:10
8:12
8:13
8:14
8:16
8:16
8:18
8:19
8:20
8:21
8:22
8:24
8:24
8:26
8:26
8:27
8:28
8:29
Actual
Tons
Loaded
12.70
10.28
21.13
11.74
11.32
21.28
12.21
12.12
12.75
12.90
12.42
12.38
12.36
12.30
12.66
12.62
12.34
12.87
12.00
12.38
20.95
13.00
12.70
13.84
14.00
21.40
12.00
12.25
12.76
13.00
13.00
12.56
11.56
12.48
21.38
12.00
12.23
13.00
12.71
13.03
13.13
12.05
Silo
No.
2
2
2
2
2
2
2
2
2
2
2
2
2
2
2
2
2
2
2
2
2
2
2
2
2
2
2
2
2
2
2
2
2
2
2
2
2
2
2
2
2
4
T-V-3 (1-4)
3-Load Out
7/27/1998
P.S. Murowchick
Derek Hawkes
T-MM5-3
3
3
3
3
3
3
3
3
3
3
3
3
3
3
3
3
3
3
3
3
3
3
3
3
3
3
3
3
3
3
3
3
3
3
3
T-M315-3
3
3
3
3
3
3
3
3
3
3
3
3
3
3
3
3
3
3
3
3
3
3
3
3
3
3
3
3
3
3
3
3
3
3
3
T-M18-3
3
3
3
3
3
3
3
3
3
3
3
3
3
3
3
3
3
3
3
3
3
3
3
3
3
3
3
3
3
3
3
3
3
3
3
final.xls
09/28/98
-------
Hot Mix Asphalt Plant C Load-Out Data
Data used in TED Emission Calculations
Client/Source
EPA Plant C
Hot Mix Asphalt
Run No
Dale:
Data Collected By:
Spreadsheet work:
Time
Of
Loading
8:30
8:32
8:33
8:34
8:35
8:37
8:38
8:39
8:40
8:41
8:42
8:43
8:44
8:45
8:47
8:48
8:49
8:51
8:52
8:53
8:54
8:55
8:56
8:58
8:59
9:00
9:01
9:02
9:02
9:03
9:04
9:06
9:07
9:08
9:08
9:10
9:10
9:12
9:14
9:15
9:16
9:17
Actual
Tons
Loaded
12.67
21.37
12.78
12.88
21.18
13.00
13.16
12.93
12.47
21.36
3.36
17.94
12.80
13.04
13.00
12.96
21.12
21.33
13.00
13.13
11.59
12.86
21.31
20.44
13.14
11.47
13.00
13.01
13.05
11.05
21.28
12.00
11.19
12.94
12.61
12.20
12.26
21.28
21.37
12.12
13.52
12.50
Silo
No.
4
4
4
4
4
4
4
4
4
4
4
5
2
2
2
2
2
2
2
2
2
2
2
2
2
2
2
2
2
2
2
2
2
2
2
2
2
2
2
2
2
2
T-V-3 (1-4)
1
3-Load Out
7/27/1998
P.S. Murowchick
Derek Hawkes
T-MM5-3
3
3
3
3
3
3
3
3
3
3
3
3
L_ 3
3
3
3
3
3
3
3
3
3
3
3
3
3
3
3
3
3
3
3
3
3
3
3
3
3
3
3
3
3
T-M315-3
3
3
3
3
3
3
3
3
3
3
3
3
3
3
3
3
3
3
3
3
3
3
3
3
3
3
3
3
3
3
3
3
3
3
3
3
3
3
3
3
3
3
T-M18-3
3
3
3
3
3
3
3
3
3
3
3
3
3
3
3
3
3
3
3
3
3
3
3
3
3
3
3
3
3
3
3
3
3
3
3
3
3
3
3
3
3
3
final.xls
09/28/98
-------
Hot Mix Asphalt Plant C Load-Out Data
Data used in TED Emission Calculations
Client/Source
Time
Of
Loading
9:19
9:21
9:23
9:26
9:27
9:29
9:31
9:32
9:33
9:34
9:35
9:37
9:38
9:39
9:43
9:44
9:45
9:46
9:47
9:51
9:52
9:53
9:54
9:57
9:58
10:00
10:03
10:04
10:05
10:06
10:07
10:07
10:09
10:09
10:11
10:11
10:12
10:14
10:15
10:16
10:17
10:20
EPA Plant C
Hot Mix Asphalt
Actual
Tons
Loaded
12.63
12.35
12.09
12.77
12.77
21.36
13.00
12.71
13.00
14.74
21.49
12.74
12.05
12
12.51
13.00
12.72
12.00
13.18
12.65
13.23
13.12
13.27
8.02
21.26
21.07
13.00
13.08
12.86
12.92
12.00
12.42
11.69
12.64
13.00
12.93
13.00
12.22
12.61
12.17
13.00
12.86
Silo
No.
2
2
2
2
2
2
2
2
2
2
2
2
2
2
2
2
2
2
2
2
2
2
2
1
2
2
2
2
2
2
2
2
2
2
2
2
2
2
2
2
2
2
Run No
Date-
3-Load Out
7/27/1998
Data collected By P.S. Murowchick
Spreadsheet wortc
T-V-3 (1-4)
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
2
2
2
2
2
2
2
2
2
2
Derek Hawkes
T-MM5-3
3
3
3
3
3
3
3
3
3
3
3
3
3
3
3
3
3
3
3
3
3
3
3
3
3
3
3
3
3
•20
final.xls
T-M315-3
3
3
3
3
3
3
3
3
3
3
3
3
3
3
3
3
3
3
3
3
3
3
3
3
3
3
3
3
3
T-M18-3
3
3
3
3
3
3
3
3
3
3
3
3
3
3
3
3
3
3
3
3
3
3
3
3
3
3
3
3
3
3
09/28/98
-------
Hot Mix Asphalt Plant C Load-Out Data
Data used in TED Emission Calculations
Client/Source
EPA Plant C
Run No.
Date:
Hot Mix Asphalt Data Collected By:
Spreadsheet work:
Time
Of
Loading
10:21
10:22
10:23
10:25
10:25
10:26
10:27
10:08
10:29
10:30
10:31
10:32
10:34
10:35
10:37
10:39
10:39
10:43
10:43
10:45
10:47
10:49
10:50
10:51
10:52
10:54
10:56
10:57
10:59
11:00
11:01
11:03
11:07
11:08
11:09
11:10
11:11
11:13
11:13
11:18
11:18
11:21
Actual
Tons
Loaded
12.79
11.73
21.25
12.82
12.90
13.00
L 13.14
20.98
8.95
12.40
13.00
13.10
21.25
21.29
21.40
13.01
12.69
12.80
12.48
21.39
21.38
13.00
12.76
21.21
21.44
12.79
12.73
21.61
12.86
12.72
20.87
21.30
12.91
12.83
21.45
11.50
10.97
12.68
15.23
12.00
11.26
12.00
Silo
No.
2
2
2
2
2
2
2
2
2
5
2
2
5
5
5
5
5
5
5
5
5
2
2
2
2
2
2
2
2
2
2
2
2
2
2
2
2
2
2
2
2
2
T-V-3 (1-4)
2
2
2
2
2
2
2
2
2
2
2
2
3
3
3
3
3
3
3
3
3
3
3
3
3
3
3
3
3
3-Load Out
7/27/1998
P.S. Murowchick
Derek Hawkes
T-MM5-3
3
3
3
3
3
3
3
3
3
3
3
3
3
3
3
3
3
3
3
3
3
3
3
3
3
3
3
3
3
3
3
3
3
3
3
3
3
3
3
3
3
3
T-M315-3
3
3
3
3
3
3
3
3
3
3
3
3
3
3
3 .
3
3
3
3
3
3
3
3
3
3
3
3
3
3
3
3
3
3
3
3
3
3
3
3
3
3
3
T-M18-3
3
3
3
3
3
3
3
3
3
3
3
3
3
3
3
3
3
3
3
3
3
3
3
3
3
3
3
3
3
3
3
3
3
3
3
3
3
3
3
3
3
3
flnal.xls
09/28/98
-------
Hot Mix Asphalt Plant C Load-Out Data
Data used in TED Emission Calculations
Client/Source
EPA Plant C
Run No.
Date
Hot Mix Asphalt Data Collected By-
Spreadsheet work.
Time
Of
Loading
11:21
11:22
11:23
11:25
11:28
11:29
11:31
11:33
11:33
11:34
11:35
• 11:36
11:36
11:37
11:38
11:39
11:41
11:41
11:42
11:43
11:44
11:45
11:47
11:48
11:49
11:50
11:51
11:51
11:52
11:54
11:55
Total
Actual
Tons
Loaded
13.22
13.00
12.78
24.53
13.00
12.92
13.00
12.73
12.00
12.91
12.00
12.56
13.00
13.60
13.00
13.14
13.00
12.67
13.00
13.10
12.00
12.49
13.00
12.96
13.00
12.46
12.50
12.31
21.08
12.00
12.64
2799.06
Silo
No.
2
2
2
2
2
2
2
2
2
2
1
1
2
2
2
2
2
2
2
2
2
2
2
2
2
2
2
2
1
2
2
T-V-3 (1-4)
3
3
3-Load Out
7/27/1998
P.S. Murowchick
Derek Hawkes
T-MM5-3
3
3
3
3
3
3
3
3
3
3
3
3
3
3
3
3
3
3
3
3
3
3
3
3
3
3
3
3
3
3
3
2530.2
T-M315-3
3
3
3
3
3
3
3
3
3
3
3
3
3
3
3
3
3
3
3
3
3
3
3
3
3
3
3
3
3
3
3
2529.7
T-M18-3
3
3
3
3
3
3
3
3
3
3
3
3
3
3
3
3
3
3
3
3
3
3
3
3
3
3
3
3
3
3
2530.2
final.xls
09/28/98
-------
APPENDIX B.4
LOAD-OUT RECORDS FOR 6/18/98 THROUGH 7/26/98
-------
ASPHALT PLANT U
HISTORICAL LOAD-IN DATA
6/18/98
6/18/98
6/18/98
6/18/98
6/18/98
6/18/98
6/18/98
6/18/98
6/18/98
6/18/98
6/18/98
6/18/98
6/18/98
6/19/98
6/19/98
6/19/98
6/19/98
6/19/98
6/19/98
6/19/98
6/19/98
6/19/98
6/19/98
6/19/98
6/20/98
6/20/98
6/20/98
6/20/98
6/20/98
6/20/98
6/20/98
6/20/98
6/20/98
6/20/98
6/20/98
rHJ^ ^OMS&HTOSF j: t* \; ^
j'is'Fv-j^f" Nsurre *- ^ '$\
ONYX Paving co, Inc.
Griffith Co.
Hillcrest Contracting
Hillcrest Contracting
City Of Dana Point
Calfon Construction, Inc.
Sequel Contractors Inc.
Silverado Constructors
Meyer E.J. Company
Copp Contracting Inc.
Damon Construction Inc.
Copp Contracting Inc.
Copp Contracting Inc.
DBL Contruction
Copp Contracting Inc.
DBL Contruction
City Service Contracting
City Service Contracting
Silverado Constructors
Silverado Constructors
Meyer E.J. Company
Calfon Construction, Inc.
Damon Construction Inc.
City Of Dana Point
Hillcrest Contracting
Far West Paving and Sealing
South Western Paving Co.
Cash Account
Seal Black
Parker Engineering
Parker Engineering
Asphalt Management Inc.
Asphalt Management Inc.
City Service Contracting
Silverado Constructors
Customer i
Nurobel i
1513
707
| 837
837
317
497
2068
2064
1323
478
402
478
478
433
478
433
341
. 341
2064
2064
1323
497
402
317
837
617
2057
1320
1968
1697
1697
642
642
341
2064
Order*
19
20
25
26
30
33
35
47
52
58
59
60
62
9
10
31
35
35
39
40
43
44
47
48
9
10
11
12
13
14
15
21
21
24
28
,O«ter
ArmwBt (Tons)
250
345
300
500
70
42
15
2,500
50
50
150
25
50
400
100
350
37
12
1,800
2,200
50
42
100
70
50
350
400
42
100
25
£.'Cl
200
100
15
2,800
13,615
ProdwIfGJt
Ra&CTPIf
75
75
125
*
*
*
*
350
50
25
25
*
*
150
*
175
*
*
300
350
50
*
*
i.
*
100
75
*
50
*
*
75
50
15
400
MB?
1 Type
1/2"
3/4"
1/2"
3/4"
3/4"
3/4"
3/4"
3/4"
3/4"
3/4"
3/4"
3/4"
3/4"
3/4"
1/2"
3/4"
3/4"
3/8"
3/4"
3/4"
1/2"
3/4"
3/4"
3/4"
3/8"
3/4" _j
3/8"
3/8"
1/2"
3/8"
3/8"
3/4"
1/2"
1/2"
3/4"
Product
Type -\
1004 III C3 AR-4000
1004 III C3 AR-4000
1004 III C3 AR-4000
1002 III B3 AR-4000
1 024 Type B AR-4000
1002 I II B3 AR-4000
1002 III B3 AR-4000
1 024 Type B AR-4000
1004 III C3 AR-4000
1001 III B2 AR-4000
1002 III B3 AR-4000
1001 III B2 AR-4000
1001 III B2 AR-4000
1 002 III B3 AR-4000 j
1004 III C3 AR-4000
1002 III B3 AR-4000
1002 III B3 AR-4000
1010 HID AR-4000
1 024 Type B AR-4000
1 024 Type B AR-4000
1004 III C3 AR-4000
1002111 B3 AR-4000
1002 III B3 AR-4000
1 024 Type B AR-4000
1010 III D AR-4000
1011 Class B AR-4000
1010 HID AR-4000
101 OHIO AR-4000
101 8 fine AR-4000
1010 III D AR-4000
101 QUID AR-4000
1042 III B3AR-8000
101 8 fine AR-4000
101 8 fine AR-4000
1024 Type B AR-4000
Sterling
' Time «.:
6:35
7:40
6:35
*
6:45
6:20
7:10
13:20
8:30
6:45
11:00
13:30
7:15
6:55
8:00
8:00
7:30
17:35
13:20
13:20
6:45
6:45
7:20
6:00
7:20
8:00
7:30
7:00
9:30
7:00
11:00
7:00
15:40
* Data Unavailable
-------
ASPHALT PLANT C
Historical Load-in Data
; •;&$&:*&!
?^>$m
6/20/98
6/20/98
6/20/98
6/20/98
6/20/98
6/22/98
6/22/98
6/22/98
6/22/98
6/22/98
6/22/98
6/22/98
6/22/98
6/22/98
6/22/98
6/22/98
6/22/98
6/22/98
6/23/98
6/23/98
6/23/98
6/23/98
6/23/98
6/23/98
6/23/98
6/23/98
6/23/98
6/23/98
6/23/98
6/24/98
6/24/98
6/24/98
6/24/98
6/24/98
6/24/98
&&i<&£ .VCwstoawr f ^
W'v^1 oNarne v -1 V
Snyder Langston Inc.
Snyder Langston Inc.
Western Paving Contract
Griffith Co.
Copp Contracting Inc.
Seal Black
Damon Construction Co.
Hillcrest Contracting
Griffith Co.
Silverado Constructors
Gansek Construction
Copp Contracting Inc.
Meyer E.J. Company
Silverado Constructors
City Of Dana Point
Calfon Construction, Inc.
Silverado Constructors
Damon Construction Co.
Hillcrest Contracting
Griffith Co.
Damon Construction Co.
Damon Construction Co.
Silverado Constructors
Calfon Construction, Inc.
Peterson-Chase Gen'l En.
Seal Black
City Of Dana Point
Copp Contracting Inc.
Meyer E.J. Company
Griffith Co.
Hillcrest Contracting
DBL Construction
Silverado Constructors
Calfon Construction, Inc.
£«$tO?n$f
*WuiN$m.
1964
1964
2332
707
478
1968
402
837
707
2064
721
478
1323
2064
317
497
2064
402
837
707
402
402
2064
497
2719
1968
317
478
1323
707
837
433
2064
497
202
jp*tor*:
«< , j
29
29
30
31
32
9
16
17
18
20
27
28
29
30
36 j
37
38
45
9
10
17
17
19
21
23
25
33
35
36
10
11
26
27
32
36
- < Order
&mobi»l{r«n$)i
200
30
345
75
50
1,400
1,300
1,500
2,500
30
75
50
40
70
42
600
150
1,875
1,600
500
600
1,300
42
150
300
70
50
50
750
550
1,000
2,100
42
150
19,611
fVsKfcKstlor*
1WWIW&
125
15
75
50
175
175
250
400
30
50
40
*
100
25
175
250
150
150
200
50
75
50
150
125
300
*
25
Mi*
J3BLJ
1/2"
1/2"
3/4"
1/2"
1/2"
rubber
3/4"
3/4"
3/4"
3/4"
1/2"
1/2"
3/4"
3/4"
3/4"
3/4"
3/4"
3/4"
1/2"
rubber
1/2"
perm
3/4"
3/4"
1/2"
3/4"
1/2"
1/2"
1/2"
3/4"
3/4"
3/4"
3/4"
1/2"
' PFQ&ft* J
Type -\
1044 III C3AR-8000
1004 III C3AR-4000
1002 III B3AR-4000
1004 III C3AR-4000
1018fineAR-4000
1032ARHM-GG-C
1002 III B3AR-4000
1002 III B3 AR-4000
Type B AR-4000
Type B AR-4000
1004 III C3 AR-4000
1004 III C3 AR-4000
Type B AR-4000
Type B AR-4000
1002 III B3 AR-4000
Type B AR-4000
1002 III B3 AR-4000
1002 III B3 AR-4000
1002 III B3 AR-4000
1032ARHM-GG-C
1004 III C3 AR-4000
1039 A.T.P.B. AR-8000
1002 III B3 AR-4000
1 524 Type B AR-4000
101 8 fine AR-4000
1024 Type B AR-4000
1004 III C3 AR-4000
1004 III C3 AR-4000
1004 III C3 AR-4000
1001 III B2 AR-4000
1002 III B3 AR-4000
1 024 Type B AR-4000
1002 III B3 AR-4000
1004 III C3 AR-4000
^arftag
*^Tim« :
7:30 AM
3:00 PM
8:40 AM
6:40 AM
6:45 AM
6:15 AM
6:55 AM
6:35 AM
5:35 PM
9:20 AM
6:40 AM
1:25 PM
10:45 AM
6:45 AM
9:20 AM
9:40 AM
6:45 AM
6:25 AM
6:35 AM
6:15 AM
6:15 AM
5:35 PM
10:20 AM
7:40 PM
7:15 AM
6:45 AM
6:40 AM
1:25 PM
6:40 AM
6:25 AM
7:30 AM
5:35 PM
10:20 AM
7:50 AM
* n««o I Inavailahta
-------
ASPHALT PLANT C
Historical Load-in Data
^U*«L*
;ifl~vi
6/24/98
6/24/98
6/24/98
6/24/98
6/24/98
6/24/98
6/25/98
6/25/98
6/25/98
6/25/98
6/25/98
6/25/98
6/25/98
6/25/98
6/25/98
6/25/98
6/25/98
6/25/98
6/26/98
6/26/98
6/26/98
6/26/98
6/26/98
6/26/98
6/26/98
6/26/98
6/26/98
6/26/98
6/26/98
6/26/98
6/26/98
6/26/98
6/29/98
6/29/98
6/29/98
f~|¥\t' J C*H*w*»Bf -^ \.
*$*!"*' %*ON»n»' x
Damon Construction Co.
Copp Contracting Inc.
Copp Contracting Inc.
Brutoco Engineering
Brutoco Engineering
Anchor Paving
DBL Construction
Copp Contracting Inc.
City Of Dana Point
Calfon Construction Inc.
Brutoco Engineering
Palomar Grading/Paving
Silverado Constructors
Griffith Co.
Ben's Asphalt
Copp Contracting Inc.
Copp Contracting Inc.
Silverado Constructors
Noble R.J.
Silverado Constructors
Silverado Constructors
Silverado Constructors
Silverado Constructors
Peterson Chase Gen'L En.
Brutoco Engineering
Brutoco Engineering
Hillcrest Contracting
Griffith Co.
Ben's Asphalt
Meyer E.J. Co.
Copp Contracting Inc.
Copp Contracting Inc.
Ben's Asphalt
Meyer E.J. Co.
City Of Dana Point
Customer
Nsmber
402
478
478
214
214
136
433
478
317
497
214
1657
2064
707
202
478
478
2064
1437
2064
2064
2064
2064
2719
214
214
837
707
202
1323
478
478
202
1323
317
Ofder#
41
43
46
54
54
55
14
26
32
33
34
35
46
50
52
56
57
58
29
41
42
42
44
30
38
38
28
35
52
59
53
54
20
21
26
\ Order -
AfRWKit'Ctons)
1,000
50
50
175
50
725
1,000
50
70
42
2,800
15
400
150
100
50
25
16
450
700
700
1,400
400
90
1,700
225
375
15
15
25
50
100
900
50
1,000
1,950
Pf*jdfcv:TMy»"
6:15 AM
8:20 AM
10:50 AM
5:30 AM
5:30 AM
*
6:30 AM
10:30 AM
*
*
5:45 AM
9:00 AM
7:35 AM
8:45 AM
6:30 AM
8:1 5 AM
1 :00 PM
12:45 PM
11:00 AM
7:40 AM
5:35 PM
5:35 PM
7:35 AM
*
5:45 AM
5:45 AM
7:00 AM
8:40 AM
6:50 AM
1:20 PM
8:30 AM
11:00 AM
7:20 AM
1:20 PM
6:45 AM
Data Unavailable
-------
ASPHALT PLANT C
HISTORICAL LOAD-IN DATA
6/29/98
6/29/98
6/29/98
6/29/98
6/29/98
6/30/98
6/30/98
6/30/98
6/30/98
6/30/98
6/30/98
6/30/98
6/30/98
6/30/98
7/1/98
7/1/98
7/1/98
7/1/98
7/1/98
7/1/98
7/1/98
7/1/98
7/1/98
7/2/98
7/2/98
7/2/98
7/2/98
7/2/98
7/2/98
7/2/98
7/2/98
7/2/98
7/2/98
7/2/98
7/2/98
j^S^v £usfcr*>er * ^ rj* ^
I'V; v^Hwto*?^ ":£
Silverado Constructors
Kajima Eng. & Const., Inc.
Copp Contracting Inc.
Copp Contracting Inc.
Silverado Constructors
Silverado Constructors
Silverado Constructors
Silverado Constructors
Excel Paving Co.
L DBL Construction
Meyer E.J. Co.
City Of Dana Point
Copp Contracting Inc.
Copp Contracting Inc.
Silverado Constructors
City Of Dana Point
Meyer E.J. Co.
Charles C. Regan Inc.
Calfon Construction, Inc.
Universal Asphalt Co. Inc.
Seal Black
Copp Contracting Inc.
Copp Contracting Inc.
Hillcrest Contracting
Silverado Constructors
Silverado Constructors
Noble R.J.
Moore Electrical Contractor
City Of Dana Point
Collins General Contractor
Silverado Constructors
Copp Contracting Inc.
City Service Contracting
Parker Engineering
Meyer E.J. Co.
^«$tort»ef':
-Hwntis*!
2064
1129
478
478
2064
2064
2064
2064
257
433
1323
317
478
478
2064
317
1323
1817
497
2105
1968
478
478
837
2064
2064
1437
1329
317
384
2064
478
341
1697
1323
StoW^
* % ">»K:
27
28
33
34
46
14
14
35
46
23
15
19
44
45
14
20
21
25
34
46
47
48 _,
49
15
33
33
36
40
41
42
43
44
47
54
57
^,~0$te£, -\
s$m&»nl Cfems.)
25
75
50
300
1,400
800
300
300
200
50
1,100
50
50
1,000
1,100
50
90
42
100
550
50
75
100
500
1,800
900
5
1,150
1,800
200
150
25
40
25
15,852
Jf^ustiprt
*
*
*
300
300
*
75
75
50
150
25
25
250
150
50
50
*
25
25
350
350
125
150
225
25
*
40
x,*!M6r"
k^V^'
1/2"
3/4"
3/4"
3/4"
3/4"
perm
3/4"
3/4"
1/2"
1/2"
rubber
3/4"
3/4"
3/4"
rubber
1/2"
1/2"
3/4"
3/8"
1/2"
3/4"
3/4"
3/4"
3/4"
perm
1/2"
1/2"
rubber
1/2"
3/4"
3/4"
3/4"
3/4"
1/2"
Product ,
t™* ---i
1004 III C3 AR-4000
1001 III B2 AR-4000
1001 III B2 AR-4000
1024 Type B AR-4000
1024 Type B AR-4000
I 1 039 AT. P. B. AR-8000
1024 Type B AR-4000
1064 Type B AR-8000
1004 III C3 AR-4000
1004 III C3 AR-4000
1032 A.R.H.M.-GG-C
1001 III B2 AR-4000
1001 III B2 AR-4000
1024 Type B AR-4000
1032 A.R.H.M.-GG-C
1004 III C3 AR-4000
101 8 Fine AR-4000
1002 III B3 AR-4000
101 OHIO AR-4000
101 8 Fine AR-4000
1001 III B2 AR-4000
1001 III B2 AR-4000
1002 III B3 AR-4000
1024 Type B AR-4000
1 039 A.T.P.B. AR-8000
1004 III C3 AR-4000
1025 Type B AR-4000
1032 A.R.H.M.-GG-C
1004 III C3 AR-4000
1024 Type B AR-4000
1001 III B2 AR-4000
1002 III B3 AR-4000
1002 III B3 AR-4000
1004 III C3 AR-4000
; Steifng
tfJ&mk •
8:30 AM
12:OOPM
7:30 AM
8:15 PM
5:35 PM
7:35 AM
6:40 PM
7:15 AM
1:20 PM
6:45 AM
10:50 AM
8:15 AM
7:40 AM
6:45 AM
1:20 PM
7:30 AM
8:50 AM
8:30 AM
1 1 :00 AM
5:35 PM
7: 15 AM
6:50 AM
6:40 AM
7:40 AM
8:20 AM
8:20 AM
10:20 AM
1-.20PM
-------
ASPHALT PLANT C
HISTORICAL LOAD-IN DATA
7/3/98
7/3/98
7/3/98
7/3/98
7/3/98
7/3/98
7/3/98
7/3/98
7/3/98
7/3/98
7/6/98
7/6/98
7/6/98
7/6/98
7/6/98
7/6/98
7/6/98
7/6/98
7/6/98
7/6/98
7/6/98
7/7/98
7/7/98
7/7/98
7/7/98
7/7/98
7/7/98
7/7/98
7/7/98
7/7/98
7/7/98
7/7/98
7/7/98
7/7/98
7/7/98
^'i ^s,^ Customer ' " -
v~\ %: ?V Name * °
Hillcrest Contracting
Silverado Constructors
Palomar Grading/Paving
Silverado Constructors
Cal-State Paving Co., Inc.
COPP Contracting Inc.
Noble R.J.
Bostic Co. J B
Snyder Langston Inc.
Collins General Contracting
Palomar Grading/Paving
Meyer E.J. Company
Russell's Site Contract
Russell's Site Contract
Russell's Site Contract
City Of Dana Point
Silverado Constructors
COPP Contracting Inc.
Hillcrest Contracting
Palomar Grading/Paving
Hillcrest Contracting
City Of Dana Point
COPP Contracting Inc.
Silverado Constructors
Far West Paving and Sealing
City of Irvine
Hillcrest Contracting
Sequel Contractors Inc.
Sequel Contractors Inc.
Western Paving Contractors
City Of Westminster
City Of Westminster
Atkinson Grading and Equip.
Gillespie Construction
Clayton Engineering Inc.
CtRifomer
Number
837
2064
1657
2064
286
478
1437
218
1964
384
1657
1323
2071
2071
2071
317
2064
478
837
1657
837
317
478
2064
617
347
837
2068
2068
2332
2305
2305
166
733
367
Order*
9
13
26
28
29
31
32
33
34
38
10
15
16
16
16
17
21
38
41
42
43
17
18
19
23
24
26
29
30
31
33
33
38
43
46
Qf&er v
AromjBt (Tana)
300
2,450
25
1,500
75
75
600
75
17
500
150
25
600
260
600
1,375
2,450
125
1,300
1,600
300
1,500
125
2,450
100
750
100
100
100
35
750
525
25
25
100
21,087
Pw$K$m
RafeCTPHJ
50
350
*
225
50
25
150
50
150
75
*
100
100
100
150
350
25
175
200
200
25
350
25
125
*
25
50
*
*
200
25
25
25
: WX
.. Type
3/4"
3/4"
3/4"
3/4"
3/8"
3/4"
3/4"
1/2"
1/2"
1/2"
1/2"
1/2"
1/2"
1/2"
3/4"
rubber
3/4"
1/2"
3/4"
1/r
1/2"
rubber
l727i
3/4"
1/2"
rubber
1/2"
3/4"
3/4"
1/2"
rubber
1/2"
3/4"
3/4"
1/2"
Product
Type , u
1002 III B3 AR-4000
1024 Type BAR-4000
1002 III B3 AR-4000
1024 Type BAR-4000
101 ONI D AR-4000
1001 III B2 AR-4000
1002 III B3 AR-4000
1004 III C3 AR-4000
1044 I II C3AR-8000
1004 III C3 AR-4000
1004 III C3 AR-4000
1004 I II C3 AR-4000
1004 III C3 AR-4000
1004 I II C3 AR-4000
1001 III B2 AR-4000
1032A.R.H.M.-GG-C
1024 Type BAR-4000
1004 I II C3 AR-4000
1002 III B3 AR-4000
1002 III B3 AR-4000
1004 III C3 AR-4000
1032A.R.H.M.-GG-C
1004 III C3 AR-4000
1024 Type BAR-4000
101 8 Fine AR-4000
1032A.R.H.M.-GG-C
1004 II! C3 AR-4000
1002 III B3 AR-4000
1002 III B3 AR-4000
1 004 III C3 AR-4000
1032A.R.H.M.-GG-C
1004 III C3 AR-4000
1002 III B3 AR-4000
1042 III B3AR-8000
1004 III C3 AR-4000
..Sterling
Time"
7:00 AM
5:35 PM
10:10 AM
7:40 AM
7:00 AM
8:30 AM
6:45 AM
6:45 AM
6:40 AM
6:40 AM
7:1 0AM
1:20 PM
7:40 AM
10:1 5 AM
6:45 AM
7:30 AM
7:35 AM
6:50 AM
6:45 AM
5:40 PM
6:1 0AM
7:30 AM
7:00 AM
10:30 AM
6:1 5 AM
10:30 AM
9:1 0AM
Data Unavailable
-------
ASPHALT PLANT C
HISTORICAL LOAD-IN DATA
7/7/98
7/7/98
7/7/98
7/7/98
7/8/98
7/8/98
7/8/98
7/8/98
7/8/98
7/8/98
7/8/98
7/8/98
7/8/98
7/8/98
7/8/98
7/8/98
7/9/98
7/9/98
7/9/98
7/9/98
7/9/98
7/9/98
7/9/98
7/9/98
7/9/98
7/9/98
7/9/98
7/9/98
7/10/98
7/10/98
7/10/98
7/10/98
7/10/98
7/10/98
7/10/98
^^iS&jNVGMiwftar ^ 3 fcV!
<*ito>.jN*to^$;rv
Meyer E J Co.
Copp Contracting Inc.
Copp Contracting Inc.
Allied Paving Co.
City Of Irvine
Copp Contracting Inc.
Tyner Paving
.Integrated Waste Management
City Of Dana Point
Silverado Constructors
City Of Westminster
City Of Westminster
Catellus Residential Co.
Catellus Residential Co.
Meyer E J Co.
Copp Contracting Inc.
Beach Paving Inc.
Hillcrest Contracting
Hillcrest Contracting
Hillcrest Contracting
City Of Dana Point
Excel Paving Co.
JES Engineering Contractors
Shamrock Asphalt
Meyer E J Co.
Meyer E J Co.
Clayton Engineering Inc.
Silverado Constructors
Silverado Constructors
Shamrock Asphalt
Hillcrest Contracting
Hillcrest Contracting
Meyer E J Co.
City Of Dana Point
Fieldstone Communities
<&$foroef i
Number!
1323
478
478
161
347
478
2017
1537
317
2064
2305
2305
153
153
1323
478 j
354
837
837
837
317
357
1006
1991
1323
1323
367
2064
2064
1991
837
837
1323
317
640
Order*
15 , ':
50
53
54
62
13
15
18
21
35
36
41
41
42
42
51
52
23
25
26
27
36
42
45
46
51
52
53
55
27
20
21
21
47
23
24
;o$*r '"v
fcni&«B^?r<*n*)
25
100
25
800
50
300
1,000
1,400
2,400
600
875
25
25
50
25
300j
900
300
300
1,400
225
115
1,200
60
60
15
600
2,000
800
1,600
500
65
1,300
850
20,340
FfO&K^R
ft«feCTP*$
*
25
125
25
75
200
150
350
150
100
50
150
100
100
175
75
150
60
60
150
300
150
225
*
60
150
175
: ; WX -;
fype\
1/2"
1/2"
3/4"
rubber
1/2"
1/2"
3/4"
rubber
3/4"
rubber
1/2"
TTz1
3/4"
1/2"
1/2"
3/8"
3/4"
1/2"
1/2"
rubber
3/4"
3/4"
172s ^
1/2" j
1/2"
3/4"
perm
1/2"
3/4"
1/2"
1/2"
rubber
374s I
'- Product • v
TV«* ^
1004 III C3 AR-4000
1004 III C3AR-4000
1002 III B3 AR-4000
1032ARHM-GG-C
1004 III C3 AR-4000
1053C2AR-8000
1002 III B3 AR-4000
1032ARHM-GG-C
1 024 Type B AR-4000
1032ARHM-GG-C
1004 III C3 AR-4000
1 025 Type B AR-4000
1024 Type B AR-4000
1004 III C3 AR-4000
1004 II I C3 AR-4000
1010 III D AR-4000
1001 III B2 AR-4000
1004 III C3 AR-4000
1004 III C3 AR-4000
1032ARHM-GG-C
1 024 Type B AR-4000
1 024 Type B AR-4000
1004 III C3 AR-4000
1004 III C3 AR-4000
1004 III C3 AR-4000
1002 III B3 AR-4000
1039A.T.P.B. AR-8000
1039 A.T.P.B. AR-8000
1004 III C3 AR-4000
1001 III B2 AR-4000
1003 III C2 AR-4000
1004 III C3 AR-4000
1032ARHM-GG-C
1 024 Type B AR-4000
$teiin8
-v-llme -•
7:20 AM
9:00 AM
7:35 AM
8:45 AM
9:30 AM
7:15 AM
6:45 AM
5:40 PM
7:10 AM
6:45 AM
1 :20 PM
7:15 AM
9:50 AM
7:10 AM
5 AM
12:00 AM
6:45 AM
7:00 AM
id AM
6:20 AM
1 :20 AM
:20 PM
>:20 AM
5:35 PM
5:40 PM
:15 AM
:35 AM
1 :20 PM
5:15 AM
i AM
* Hata Unavailable
-------
-p
ASPHALT PLANT C
HISTORICAL LOAD-IN DATA
7/13/98
7/13/98
7/13/98
7/13/98
7/13/98
7/13/98
7/13/98
7/13/98
7/13/98
7/14/98
7/14/98
7/14/98
7/14/98
7/14/98
7/14/98
7/14/98
7/14/98
7/14/98
7/15/98
7/15/98
7/15/98
7/15/98
7/15/98
7/15/98
7/15/98
7/15/98
7/15/98
7/15/98
7/15/98
7/15/98
7/16/98
7/16/98
7/16/98
7/16/98
7/16/98
^•l/' £ ^ Ou^ower- \ ' -!
'£f5r *'O Narne_ : *\ *>
Silverado Constructors
Silverado Constructors
Silverado Constructors
Sequel Contractors Inc.
Excel Paving Co.
Meyer E.J. Company
City Of Dana Point
Brutoco Engineering
Brutoco Engineering
John Laing Hones
Silverado Constructors
Silverado Constructors
Silverado Constructors
Silverado Constructors
Excel Paving Co.
Sequel Contractors Inc.
Meyer E.J. Company
Sequel Contractors Inc.
John Laing Homes
City Of Irvine
Silverado Constructors
Silverado Constructors
Bully Miller Contracting
C A Rassmussen
Silverado Constructors
Kajima Eng. And Constr.
Asphalt Care
City Of Dana Point
Hillcrest Contracting
Meyer E.J. Company
Clayton Engineering Inc.
Hillcrest Contracting
Bayley Construction
Bayley Construction
Silverado Constructors
<3fcgtwi*&r
Number
2064
2064
2064
2068
357
1323
317
214
214
1029
2064
2064
2064
2064
357
2068
1323
2068
1029
347
2064
2064
1943
483
2064
1129
2703
317
837
1323
367
837
247
247
2064
Order #
24
27
27
35
15
36
22
21
21
18
21
23
25
25
30
32
34
37
15
18
19
20
21
22
23
24
37
40
43
44
19
22
25
25
26
, OWler
Arr«sff*t(T0ns):
2,^100
120
300
75
1,600
65
1,175
500
75
500
3,200
75
1,100
150
650
200
75
200
475
800
3,200
1,000
15
1,100
300
12
25
50
100
86
10
900
75
1,600
300
22,508
Pfodut$0rt
Ra&CTPHI
325
50
*
50
250
75
175
*
125
150
450
*
175
175
150
50
75
50
150
125
450
*
*
250
50
*
*
*
175
*
*
150
200
200
50
: MS*
, Type
3/4"
3/4"
3/8"
3/4"
3/4"
1/2"
rubber
1/2"
3/4" j
1/2"
3/4"
perm
3/4"
perm
3/4"
3/4"
1/2"
3/4"
1/2"
rubber
3/4"
3/4"
3/8"
3/4"
perm
3/4"
1/2"
1/2"
3/4"
1/2"
3/4"
3/4"
3/4"
1/2"
berm
Product i
: Type ^ \
1 024 Type BAR-4000
1 024 Type B AR-4000
1066 Type BAR-8000
1002 III B3 AR-4000
1024 Type BAR-4000
1004 III C3 AR-4000
1032ARHM-GG-C
1053C2AR-8000
1051 BAR-8000
1004 III C3 AR-4000 _,
1024 Type BAR-4000
1066 Type BAR-8000
1024 Type BAR-4000
1039A.T.P.B. AR-8000
1024 Type BAR-4000
1002 III B3 AR-4000
1004 III C3 AR-4000
1002 III B3 AR-4000
1004 III C3 AR-4000
1032ARHM-GG-C
1024 Type BAR-4000
1024 Type BAR-4000
1026 Type BAR-4000
1001 III B2 AR-4000
1066 Type BAR-8000
1002 III B3 AR-4000
101 8 Fine AR-4000
1004 III C3 AR-4000
1002 III B3 AR-4000
1004 III C3 AR-4000
1002 III B3 AR-4000
1002 III B3 AR-4000
1024 Type BAR-4000
1025 Type BAR-4000
1066 Type BAR-8000
Starting
Time "
5:40 PM
8:40 AM
*
10:15 AM
7:00 AM
1:20 PM
6:45 AM
*
5:30 AM
7:40 AM
5:48 PM
*
8:40 AM
7:40 AM
7:00 AM
*
1:20 PM
*
7:36 AM
*
5:40 PM
1 :40 PM
12:15 AM
6:45 AM
7:40 AM
*
9:30 AM
*
*
1:20 PM
7:30 AM
7:05 AM
6:30 AM
6:50 AM
7:40 AM
* Data Unavailable
-------
ASPHALT PLANT C
HISTORICAL LOAD-IN DATA
^V^!^
7/16/98
7/16/98
7/16/98
7/16/98
7/16/98
7/16/98
7/20/98
7/20/98
7/20/98
7/20/98
7/20/98
7/20/98
7/20/98
7/21/98
7/21/98
7/21/98
7/21/98
7/21/98
7/21/98
7/21/98
7/21/98
7/21/98
7/21/98
7/21/98
7/21/98
7/21/98
7/22/98
7/22/98
7/22/98
7/22/98
7/22/98
7/22/98
7/22/98
7/22/98
7/22/98
i$,$ j%;ott»fo**r: /v \
pP-fC ^> Nsiw' x% ""
City of Dana Point
Silverado Constructors
Silverado Constructors
Silverado Constructors
C. A. Rassmussen
Ahmadi M. Const. And Eng.
Silverado Constructors
Brutoco Engineering
Brutoco Engineering
Pave West Inc.
Sequel Contractors Inc.
Copp Contracting Inc.
Copp Contracting Inc.
GMC Enterprises
Hillcrest Contracting
Copp Contracting Inc.
Hillcrest Contracting
Allied Paving Co.
Pave West Inc.
Avafa and Sons, Inc.
Avala and Sons, Inc.
Irvine Company, The
Irvine Company, The
Meyer E. J. Company
Silverado Constructors
Silverado Constructors
Silverado Constructors
Pave West Inc.
Western Paving Contract
Allied Paving Co.
Western Paving Contract
Preferred Paving
Myles Construction
Meyer E. J. Company
Hillcrest Contracting
<&$iprf*$r
Number i
317
2064
2064
2064
483
850
2064
214
214
1679
2068
478
478
711
837
478
837
161
1679
128
128
909
909
1323
2064
2064
2064
1679
2332
161
2332
1618
1305
1323
837
Qrde?$
\ ^ * *
33
34
34
35
39
49
38
24
24
17
44
20
21
9
10
11
14
15
16
17
17
21
21
40
41
44
26
27
25
46
44
28
82
17
49
- Qflta^
^ArraHadl ££oni>
50
500
1,200
3,200
125
6
2,400
125
250
1,500
2,000
291
650
275
75
280
25
400
1,500
200
850
1,225
400
50
2,400
90
800
1,500
900
25
4
700
475
80
75
24,626
Pft^UStliprj
f&te(T!»Hjl
50
250
250
450
50
*
350
*
175
175
200
*
125
50 _,
*
125
*
100
175
100
175
225
*
50
400
90
150
175
150
•*
*
50
*
80
*
:'; Mix ,
: Type -
1/2"
perm
3/4"
3/4"
1/2"
3/4"
3/4"
1/2"
3/4"
1/2"
1/2"
1/2"
1/2"
3/4"
3/4"
1/2"
1/2"
1/2"
1/2"
1/2"
rubber
3/4"
1/2"
1/2"
3/4"
1/2"
3/4"
1/2"
1/2"
3/4"
1/2"
3/8"
1/2"
1/2"
3/4"
Proditd; V-;v
\ > Tyffe > * * 7r
1004 I II C3 AR-4000
1039A.T.P.B. AR-8000
1024 Type B AR-4000
1024 Type B AR-4000
1004 III C3 AR-4000
1524 TypeB AR-4000
1 024 Type B AR-4000
1053 C2 AR-8000
1051 B AR-8000
1044 III C3 AR-8000
1004 III C3 AR-4000
1004 III C3 AR-4000
1004 III C3 AR-4000
1002 III B3 AR-4000
1002 III B3 AR-4000
1004 III C3 AR-4000
1004 III C3 AR-4000
1010 Fine AR-4000
1044 III C3 AR-8000
1004 III C3 AR-4000
1032 ARHM-GG-C
1002 III B3 AR-4000
1004 III C3 AR-4000
1004 III C3 AR-4000
1024 TypeB AR-4000
1025 TypeB AR-4000
1024 TypeB AR-4000
1044 III C3 AR-8000
1044 III C3 AR-8000
1002 III B3 AR-4000
1044 III C3 AR-8000
1010 HID AR-4000
1003 III C2 AR-4000
1044 III C3 AR-8000
1002 III B3 AR-4000
^Sterling
l>,ti«*e
7:15 AM
5:40 PM
7:40 PM
*
7: 15 AM
7:10 AM
5:35 PM
*
5:45 AM
5:00 AM
6:40 AM
*
7:25 AM
7:00 AM
6:25 AM
7:25 AM
*
6:50 AM
5:00 AM
8:30 PM
10:30 PM
6:20 AM
*
1:50 PM
5:35 PM
6:05 AM
7:35 AM
5:00 AM
6:50 AM
9:50 AM
1:00 AM
6:40 AM
*
12:55 PM
7:50 AM
-------
ASPHALT PLAN I u
HISTORICAL LOAD-IN DATA
M>t
7/22/98
7/23/98
7/23/98
7/23/98
7/23/98
7/23/98
7/23/98
7/23/98
7/23/98
7/23/98
7/23/98
7/24/98
7/24/98
7/24/98
7/24/98
7/24/98
7/24/98
7/24198
7/24/98
7/24/98
7/24/98
7/24/98
7/24196
7/24/98
7/25/98
7/25196
7/25/98
7/25/98
Kfc^'-C-uSJ&wieSS. - W
«!K * #B«* J *~-
Hillcrest Contracting
Ayala & Sons, Inc.
Ayala & Sons, Inc.
Hillcrest Contracting
Meyer E. J. Company
Hillcrest Contracting
Haitbrink Asphalt Paving
Anchor Paving
Hillcrest Contracting
Mission Paving
Silverado Constructors
Hillcrest Contracting
Hillcrest Contracting
Ben's Asphalt
Ayala & Sons, Inc.
Ayala & Sons, Inc.
Silverado Constructors
Silverado Constructors
Presley Company
Excel PavinsCo.
Clayton Engineering Inc.
Silverado Constructors
Snyder Langston Inc.
Snyder Langston Inc.
Silverado Constructors
Silverado Constructors
Silverado Constructors
Ben's Asphalt
Cifetonie*
C$tlffl€Htt\
837
128
128
837
1323
837
852
136
837
1315
2064
837
837
202
128
128
2064
2064
1605
357
367
2064
1964
1964
2064
2064
2064
202
^^V?*'* ^>\
20
10
10
12
14
17
18
20
23
26
29
10
15
16
27
27
30
31
L_ 33
47
48
49
50
62
18
19
20
12
Total for 6/29/98 - 6/29/98, used in sum 6/29/98 to 7/25/98 below
Total for 6/29/98 - 7/2/98, used in sum 6/29/98 to 7/25/98 below
Total for 7/3/98 - 7/7/98, used in sum 6/29/98 to 7/25/98 below
Total for 7/7/98 - 7/10/98, used in sum 6/29/98 to 7/25/98 below
"otal for 7/13/98 - 7/16/98, used in sum 6/29/98 to 7/25/98 below
Total for 7/1 6/98 - 7/22/98, used in sum 6/29/98 to 7/25/98 below
Total for 7/23/98 - 7/25/98, used in sum 6/29/98 to 7/25/98 below, also see Note
Total for 6/29/98 - 7/25/98, used below, see Notes 2 & 3
Total for 7/19/98 - 7/22/98, used to calculate 7/19/99 to 7/25/98
Total for 7/1 9/98 - 7/25/98, used below, see Note 4
Used in the TED Deposition Calcualtion
Used in the Ceiling Deposition Calculation
Used in the Exhaust Plenum Calculation POX pipe)
Used in the New SED Deposition Calculation
; 7«i*Bfer
-Amoo^f&ws)
500
850
200
75
80
1,300
250
40
50
800
2,400
75
800
200
850
200
2,800
2,400
1,275
15
25
84
82
175
2,400
250
2,800
190
1,950
15,852
21,087
20,340
22,508
24,626
20,666
125,079
19,545
40,211
75,047
20,666
4,133
8,042
JPto&fcb&ft
^m&w
125
175
100
*
80
175
75
25
*
100
400
*
175
*
175
100
400
250
125
*
21
*
25
85
300
300
400
100
Mix
Typ»
1/2"
•
*
*
*
•
•
*
*
*
*
3/4"
1/2"
1/2"
rubber
1/2"
3/4"
3/4"
3/4"
1/2"
1/2"
3/4:"
1/2"
*
3/4"
3/4"
3/4"
1/2"
•^ pfcefeef '; ;"'
Type: " 5" '
1004 III C3AR-4000
1032ARHM-GG-C
1004 III C3AR-4000
1002 III B3AR-4000
1004 III C3AR-4000
1002 III B3AR-4000
1004 III C3AR-4000
1018FineAR-4000
1004 III C3AR-4000
1018FineAR-4000
1024 Type BAR-4000
1002 III B3AR-4000
1004 III C3AR-4000
1018FineAR~4000
1032ARHM-GG-C
1004 III C3AR-4000
1 024 Jypjj BAR-4000
1024 Type BAR-4000
1002 III B3AR-4000
1004 III C3AR-4000
1004 III C3AR-4000
1024 Type BAR-4000
1043 III C2AR-8000
1025 Type BAR-4000
1024 Type BAR-4000
1024 Type BAR-4000
1024 Type BAR-4000
1018 Fine AR-4000
4^ ^Sfeirtins ^
?tefr 'J&A^
6:50 AM
*
•
7:50 AM
9:20 AM
7:05 AM
8:50 AM
10:50 AM
7:1 5 AM
6:15 AM
5:35 PM
7:50 AM
6:45 AM
*
10:20 PM
8:20 PM
5:35 PM
6:35 AM
6:40 AM
6:45 AM
6:1 5 AM
6:35 AM
11:35 AM
•
6:40 AM
7:40 AM
5:40 PM
6:1 5 AM
See note 1 below
See note 2 below
See note 3 below
See note 4 below
NOTES:
1 TED Test plates were Installed from 6729/98 thru 7/25/98. Total production during that time was 125,079. Test plates were exposed to load-out from 3 of 5 silos. Three fifths of 125,079 equals 75,347
2 Ceiling plates were installed from 7/23/98 thru 7/25/98; Total production during that time was 20,666
3 Box pipe were installed from 7/23/98 (tiru 7/25/98; Total production during that time was 20,666. Box pipe were exposed in only one silo. One fifth of 20,666 equals 4,133
4 New SED w«» installed from 7/19/98 thru 7/25/98; Total production during that time was 40.711. SED was exposed in only one silo. One fifth of 40,711 equals 8,142
' Data Unavailable
-------
APPENDIX B.5
LOAD-OUT RECORDS FOR 7/24/98 THROUGH 7/28/98
-------
4-5"
-------
Load-Out Log Spreadsheet
Sheet
of 5"~
MProiwtNo. 4701-08-03-04
RUT NO. / - Load Ovf
Hoi- /tf/y
OtURMontodBy:
Product
ID
Product Description
Job
Name
Time
Of
Loadng
Actual
Tons
Loaded
Truck
No
33
TZT
3/
77/7
r?
foo1/
iff. £3
/to?
20.63
toff
(00)*-
fn
33
£0.10
13
*, vA
ZL
lod
0152-
/£»/
3/
/(*
/
JLI
d 3
XT
^f,/-,
g/^oj
to
mri fites\ftirfonn\ProductionData
Midwest RttseAich Institute
-------
Load-Out Log Spreadsheet
Sheet ^ of
41
mri fll«s\ftirfonn\PR>ductionOa1a
Midwwt R«MWch Imtitiite
07M3A8
-------
Load-Out Log Spreadsheet
Sheet
Mr*Pn*ctto. 4701-M-03-O4
RunNe
/ - IJHZO/ OtS T-
Proouct
10
Product OeMripten
Job
Name
Thm
Of
Loadtng
ActMl
Tom
Loaded
Tiuck
No
Slo
No.
MX
Tamp.
to Truck
Commwits
w
(,0
33
look
3/
fool
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/o II
too1/
IS'
tail
GL.
3 /
3-1.
3 /
too*
B3
0%
?
OM.
7Z7"£?
4*
-------
Load-Out Log Spreadsheet
4701-QMO-M
tfof
Q3
Name
/r
Of
Lowing
Tom
Loaded
Truck
No
Sto
No.
Ma
Temp.
In Truck
Comments
to
up* 6
Ti
/oo
-2/7
G
ll
25?
**/''
3/
B
//53
aj.Bf
too
If.51
TI£ 53
If
/r
-------
Load-Out Log Spreadsheet
Sheet 5"of
**PK«M»NO. 4701-M-03-0*
/H,Y
Product
to
Product DeMrtpten
Job
Name
Tbrw
Of
.oadno
Actual
Tom
Tnicfc
No
Sto
No.
Mix
Tamp.
In Truck
ComnMnts
/3
33
100 "/
3/
100*-
(003-
/oo*.
. 37
53
O/
3/
31.
i, n
±L
nvri
-------
T/L
tool/ 7/T
ff
/
3-(j> /O
-------
Load-Out Log Spreadsheet
Sheet
Mn Pr<»«a No. ^701-08-03-04
ClwntSoure*:
A* 0hGjLf-
Run No.
DM*:
D«tl R«cord«d By:
ID
Product Description
Name
Time
Of
Loading
Actual
Tons
Loaded
Truck
No
Sfe
No.
Mix
Temp.
in Truck
Comments
**/.
III (13 At-Vooo
A
If
01 (^
5"
27 gj
B V"
(to
A
nt'rf
-------
Load-Out Log Spreadsheet
Sheet <9v i
MrtPro^aNo. 4701-08-03-04
CKwitfSoufc*:
(L
'Ms*
Run No.
DM:
DM R*cort«d By:
ID
ob
Name
Time
Of
Loading
Actual
Tons
Loaded
Truck
No
SSo
No.
Mix
Temp.
in Truck
Comments
6 3/
2222
\
if
(1
A?
n
?
-------
Load-Out Log Spreadsheet
Sheet
E
4701-08-03-04
MM As /?/W/
M.R.eortMBy:
/ft
Product
ID
Product Description
Job
Name
Time
Of
Loading
Actual
Tons
Loaded
Truck
No
sao
No.
Temp.
in Truck
Comments
/OPS/
03/0
3/PSl
tooi
*'
TV* B *'
B>
/r
A
n
te
do
mri fihtstflii foi 11 i\ProductkxiOata
Midwest RnMunch Instibite
07/13/W
-------
Load-Out Log Spreadsheet
Sheet
Preset No. 4701-08-03-04
y-
Product
ID
Product Description
Job
Name
Time
Of
Loadmg
Actual
Tons
Loaded
Truck
No
S8o
No.
Mix
Temp.
in Truck
Comments
(1
if
/ft
18
(is
net
V
//
/osv
(98
to&j
/w
$00
//of
Z/.ol
*/
-------
Load-Out Log Spreadsheet
Sheet / of V.
*•/
12.
loxi
3-tjy
loot*
hrt
01/1
£7/3
01/8
fr&if
/r
•v ITT?
fro
6
35^7
{00*-
07/7
. 10
3'/**>
'A3
ro
08/3
30
fa C/C
mri fUes\fbrform\ProductionOata
Midwest Research bntiliite
07A13M
-------
Load-Out Log Spreadsheet
Sheet Z- of
*if>n*«tNo. 4701-08-03-04
CMntfSourc*
Run No.
/
C
t-h-f
CMiRKORMBy:
O C*J rJl /C /<.
Product
ID
Product Description
.lob
Name
Time
Of
Loadkig
Actual
Tons
Loaded
Truck
No
sao
No.
Mix
Temp.
in Truck
Comments
10*4
0%/lfi
/w
fy.co
08/1
76
fact.
lorf
3900
V'
/e
~ST £-
083?
£*<-/£
n
6-
?&
II
mri fite»tfBrfofm\ProdoctionOata
07/13M
-------
Load-Out Log Spreadsheet
Sheet
of "7
rfn Preset No. 4701-08-03-04
RunNo.
/
M.R.onMBy:
Product
ID
Product Description
Job
Name
Time
Of
Loading
Actual
Tons
Loaded
Truck
No
Slo
No.
Mix
Temp.
in Truck
Comments
fML
K
ro
ol
AT
/fry
0853-
it
H
-r*
if
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ctfol
II. of
of
70
/>. 00
if
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/A.*/
tin
/,
ff
ft
09/9
if
mri fitesVnirfonn\ProductkMiData
MidwMtRt
07/13«e
-------
Load-Out Log Spreadsheet
Sheet
ProfWtNo. 4701-08-03-04
RunNo.
/
(?
CMitteconMBy:
: r~>
Product
ID
Product Description
Job
Name
Time
Of
Loading
Actual
Tons
Loaded
Truck
No
Sflo
No.
Mix
Temp.
in Truck
Oomfncnts
-STA-\
front
t<
If
V
of 31
13,00
l
fact
h+'f
QO/
ff
(3
6937
n
2.
K
K
mri fitestfWrfonn\ProdtJctk>oData
MidwKt Research Institute
07/13/98
-------
Load-Out Log Spreadsheet
Sheet
* 7
CDtnVSoura:
4701-08-03-0*
DM FUcort^J Br-
Product
ID
Product Description
Job
Name
Time
Of
Loading
Actual
Tons
Loaded
Truck
No
Sto
No.
Mix
Temp.
in Truck
Comments
/Gen
(l
If
too?
to*/
V
/Off
13.00
fof/
01-
/•
tf
K
A/-?
If
ff
/on
0-*
ft
/o>4
K
II
/A73
*«"
II
K
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(
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/ft*
/f
'
loo>
, v '0
ot
i. -T
mri fitestftirfonrnProductionDati
Midvwst RMMHdi Instiluti
07/13A8
-------
Load-Out Log Spreadsheet
Sheet
4701-08-03-04 ,
0-
MiFteeoRMBy:
/fj I/SV
Product
ID
Product Description
Job
Name
Time
Of
Loading
Actual
Tons
Loaded
Truck
No
sao
Mix
Temp.
in Truck
Comments
-To A, &
K
TIL R~
/S.oo
nn
K
oo*-
o
*«/*
H
n
7ZZ"
20
/I/O
ITL
/?
06
HCto
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liio
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Ull
(037
if
n
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n
ft 15
f/
If
?*
H/8
/i
H
B
//*!
H
5
. oo
'*.!€>
mri IHcsVRiffonnVProductionOata
-------
Load-Out Log Spreadsheet
Sheet 1 of
AriPrajwtNo. 4701-08-03-04 ,
ItanVSourcr.
RunN..
Product
ID
Product Description
Job
Name
Tune
Of
Loading
Actual
Tons
Loaded
Truck
No
sao
No.
Mix
Temp.
in Truck
Comments
AW
15.00
>.?*
n
/w
/3>.oo
f/
focff
t(
n
V
"
tl
(f
r(
tr
/I
ft
ff
'3.00
//
ff
100^
20
n
ii
/i
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ff
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TTTfe
n
ff
mri filesWrformVProductionOata
or/iane
-------
->v
6:21 AM
6:27 AM
6:30 AM
6:34 AM
6:42 AM
6:46 AM
6:50 AM
6:53 AM
6:56 AM
7.22 AM
7:30 AM
7:36 AM
:39
:42
AM
AM
:44 AM
:46 AM
:48 AM
:50AM
7:55 AM
7:57 AM
8:00 AM
8:02
8:05 AM
8:07 AM
8:10AM
8:11 AM
8:16 AM
8:18 AM
8:20 AM
8:23 AM
8:25 AM
8:27 AM
8:30 AM
8:31 AM
8:33 AM
8:35 AM
8:39 AM
8:41 AM
8:43 AM
8:45 AM
8:49 AM
8:51 AM
8:53 AM
8:57 AM
8:58 AM
9:00 AM
9:01 AM
9:05 AM
9:07 AM
LOAD-OUT DATA
FOR 7/28/98
Griffith Company
Griffith Company
Griffith Company
Griffith Company
oany
pany
Griffith Company
Ivy Inc.
Silverado Constructors
Standard-Pacific Corp.
Griffith Company
Griffith Company
Hillcrest Contracting
Griffith Company
Griffith Company
Standard-Pacific Corp.
Griffith Company
Silverado Constructors^
Griffith Company ~
Griffith Company
Griffith Company
Standard-Pacific Cor
Bostick Co., J B
Griffith Company
Griffith Company
Bostick Co.. JB
Griffith Company
Griffith Company
Interstate Asphalt
Griffith Company
Griffith Company
Bostick Co., J B
Standard-Pacific Corp.
Griffith Company
Standard-Pacific Corp.
Bostick Co., J B
Griffith
Griffith Company
Bostick Co., J B
Standard-Pacific Corp.
Griffith Company
Interstate Asphalt
Standard-Pacific Corp.
Bostick Co., JB
1001
221505
102806
195512
195508
2305
3419
27
201064
201002
303502
12
102806
195512
10
2475 I 25.49 I 1024 Type B 3/4" M.M. AR-4000
27.67
25.66
25.97
24.39
11
15
3061
2475
3246
2305
44
3419
29
25.79
25.96
121415 | 25^69
— •
29
2475
1001
16
3246
2305
221505
13
15.22
25.68
27.84
21.22
24.23
25.31
25.52
21.16
102801 I 2539
25.88
23.15
103202 I 26.07
21.22
155403 I 25^9
25.75
25.43
24.44
21.19
25.75
21.2
195508 I 25.88
121415 | 25.76
19.95
1298 I 26.02
230506 | 25.15
21.32
312505 I 23.88
230506 | 25.59
21.21
24.17
21.65
25.9
27.89
21.13
24.12
25.29
21.33
24.17
24.04
1024 Type B 3/4" M.M. AR-4000
1024 Type B 3/4" M.M. AR-4000
1024 Type B 3/4" M.M. AR-4000
1024 Type B 3/4" M.M. AR-4000
1024 Type B 3/4" M.M. AR-4000
1024 Type B 3/4" M.M. AR-4000
1024 Type B 3/4" M.M. AR-4000
1024 Type B 3/4" M.M. AR-4000
1002 III B3 AR-4000
1024 Type B 3/4" M.M. AR-4000
1024 Type B 3/4" M.M. AR-4000
1066 Type B 3/8" AR-8000
1002 III B3 AR-4000
1024 Type B 3/4" M.M. AR-4000
1024 Type B 3/4" M.M. AR-4000
1002 III B3 AR-4000
1024 Type B 3/4" M.M. AR-4000
1024 Type B 3/4" M.M. AR-4000
1002 III B3 AR-4000
1024 Type B 3/4" M.M. AR-4000
1066 Type B 3/8" AR-8000
1024 Type B 3/4" M.M. AR-4000
1024 Type B 3/4" M.M. AR-4000
1024 Type B 3/4" M.M. AR-4000
1002 III B3 AR-4000
1010 HID AR-4000
24.37 I 1024 TypeB 3/4" M.M. AR-4000
1024 Type B 3/4" M.M. AR-4000
1010 HID AR-4000
1024 Type B 3/4" M.M. AR-4000
1024 Type B 3/4" M.M. AR-4000
1004 III C3 AR-4000
1024 Type B 3/4" M.M. AR-4000
1024 Type B 3/4" M.M. AR-4000
101 OHIO AR-4000
1002 III B3 AR-4000
1024 Type B 3/4" M.M. AR-4000
1004 III C3 AR-4000
1002 III B3 AR-4000
101 QUID AR-4000
1024 Type B 3/4" M.M. AR-4000
1024 Type B 3/4" M.M. AR-4000
1010 III D AR-4000
1002 III B3 AR-4000
1024
B 3/4" M.M. AR-4000
1004 III C3 AR-4000 "
1002 III B3 AR-4000
1010 HID AR-4000
-------
LOAD-OUT DATA
FOR 7/28/98
, % TH88v«£
N vH^" ™V
9:10 AM
9:14 AM
9:1 7 AM
9:19 AM
9:20 AM
9:24 AM
9:27 AM
9:29 AM
9:31 AM
9:33 AM
9:35 AM
9:37 AM
9:39 AM
9:41 AM
9:49 AM
9:51 AM
9:53 AM
9:55 AM
9:57 AM
9:59 AM
10:01 AM
10:03 AM
10:07 AM
10:09 AM
10:11 AM
10:13 AM
10:16 AM
10:18AM
10:26 AM
10:28 AM
10:36 AM
10:40 AM
10:43 AM
10:44 AM
10:48 AM
10:49 AM
10:52 AM
10:54 AM
10:57 AM
10:59 AM
11:01 AM
11:03 AM
1 1 :06 AM
11:08 AM
11:11 AM
11:13AM
11:18AM
11:19AM
.11:20 AM
,*I*Y:;£ f%388QWER%^^f\
v^^^^&s^?"?* *i
Hillcrest Contracting
Griffith Company
Griffith Company
Standard-Pacific Corp.
Standard-Pacific Corp.
Griffith Company
Interstate Asphalt
Griffith Company
Standard-Pacific Corp.
Bostick Co., J B
Griffith Company
Griffith Company
Standard-Pacific Corp.
Interstate Asphalt
Griffith Company
Griffith Company
Standard-Pacific Corp.
Bostick Co., J B
Griffith Company
Griffith Company
Interstate Asphalt
Standard-Pacific Corp.
Griffith Company
Griffith Company
Standard-Pacific Corp.
Bostick Co., J B
Interstate Asphalt
Griffith Company
Standard-Pacific Corp.
Griffith Company
Interstate Asphalt
Griffith Company
Griffith Company
Silverado Constructors
Griffith Company
Silverado Constructors
Griffith Company
Griffith Company
Interstate Asphalt
Griffith Company
Griffith Company
Griffith Company
Bostick Co., J B
Griffith Company
Griffith Company
Interstate Asphalt
Griffith Company
Griffith Company
Griffith Company
£3$$$|$
-------
LOAD-OUT DATA
FOR 7/28/98
: **&^
11:23 AM
11:25 AM
11:27 AM
11:29 AM
11:31 AM
11:33 AM
11. -35 AM
11:38 AM
11:39 AM
11:41 AM
11 :44 AM
11:50 AM
11:54 AM
11:56 AM
11:58 AM
12:00 PM
12:04 PM
12:06 PM
12:08 PM
12:09 PM
12:11 PM
12:13 PM
12:15 PM
12:17 PM
12:20 PM
12:23 PM
12:28 PM
12:30 PM
12:37 PM
12:41 PM
12:42 PM
12:45 PM
12:52 PM
12:54 PM
12:56 PM
12:59 PM
1:01 PM
1:02 PM
1:05 PM
1:08 PM
1:12 PM
1:15 PM
1:16 PM
1:20 PM
1:21 PM
1:23 PM
1:25 PM
1:29 PM
1:31 PM
i X^SSS^N. K «. *"ftr^ Jt*»*lwJC«'> J^Wx&S'"® 5;
Griffith Company
BostickCo., J B
Griffith Company
Griffith Company
Interstate Asphalt
Griffith Company
Hillcrest Contracting
Griffith Company
Bostick Co., J B
Griffith Company
Standard-Pacific Corp.
Griffith Company
Interstate Asphalt
Bostick Co., J B
Standard-Pacific Corp.
Griffith Company
Griffith Company
Standard-Pacific Corp.
Standard-Pacific Corp.
Southwest Contractors
Griffith Company
Griffith Company
Interstate Asphalt
Griffith Company
Griffith Company
Griffith Company
Griffith Company
Silverado Constructors
BostickCo., JB
Standard-Pacific Corp.
Interstate Asphalt
Standard-Pacific Corp.
Southwest Contractors
Griffith Company
Griffith Company
Standard-Pacific Corp.
Bostick Co., J B
Interstate Asphalt
Griffith Company
Standard-Pacific Corp.
Griffith Company
Griffith Company
BostickCo., J B
Interstate Asphalt
Griffith Company
Griffith Company
Bostick Co., J B
Griffith Company
Griffith Company
wjx' 1 ^$^vi VtS
195512
10
195508
1717
29
121415
13
2740
15
1298
3061
230506
312505
12
3419
230506
1001
3246
312503
9
2305
2475
312501
2305
102801
221515
201002
16
15
3188
29 _j
3061
10
221505
155403
213501
13
44
195512
3419
201064
102806
18
312503
195508
121415
12
1717
2740
sOftDED
25.9
21.24
26.01
25.75
24.59
25.72
21.22
25.58
21.22
26.13
24.1
25.68
24.08
21.45
24.48
25.16
27.72
24.16
24.04
20.14
25.47
25.7
24.56
25.91
26.23
25.78
25.6
21:09
21.23
24.36
24.53
24.1
20.02
25.65
25.57
24.32
21.33
21.12
25.81
24.71
25.79
24.59
21.63
23.79
26.16
25.91
21.28
25.57
25.64
1024 Type B 3/4" M.M. AR-4000
1010 HID AR-4000
1024 Type B 3/4" M.M. AR-4000
1024 Type B 3/4" M.M. AR-4000
1004 III C3 AR-4000
1024 Type B 3/4" M.M. AR-4000
1002 III B3 AR-4000
1024 Type B 3/4" M.M. AR-4000
1010 HID AR-4000
1024 Type B 3/4" M.M. AR-4000
1002 III B3 AR-4000
1024 Type B 3/4" M.M. AR-4000
1004 III C3 AR-4000
101 OHIO AR-4000
1002 III B3 AR-4000
1024 Type B 3/4" M.M. AR-4000
1024 Type B 3/4" M.M. AR-4000
1002 I II B3 AR-4000
1002 III B3 AR-4000
1011 Class B 3/4" AR-4000
1024 Type B 3/4" M.M. AR-4000
1024 Type B 3/4" M.M. AR-4000
1004 III C3 AR-4000
1024 Type B 3/4" M.M. AR-4000
1024 Type B 3/4" M.M. AR-4000
1024 Type B 3/4" M.M. AR-4000
1024 Type B 3/4" M.M. AR-4000
1066 Type B 3/8" AR-8000
1010 III D AR-4000
1002 III B3 AR-4000
1004 III C3 AR-4000
1002 III B3 AR-4000
1011 Class B 3/4" AR-4000
1024 Type B 3/4" M.M. AR-4000
1024 Type B 3/4" M.M. AR-4000
1002 III B3 AR-4000
1010 HID AR-4000
1004 III C3 AR-4000
1024 Type B 3/4" M.M. AR-4000
1 002 III B3 AR-4000
1024 Type B 3/4" M.M. AR-4000
1024 Type B 3/4" M.M. AR-4000
1010 HID AR-4000
1004 III C3 AR-4000
1024 Type B 3/4" M.M. AR-4000
1024 Type B 3/4" M.M. AR-4000
101 OHIO AR-4000
1024 Type B 3/4" M.M. AR-4000
1024 Type B 3/4" M.M. AR-4000
-------
LOAD-OUT DATA
FOR 7/28/98
T4ft jftC •• j-y ^ •
T t^W**- y-y-<
1 :33 PM
1:35 PM
1:37 PM
1:39 PM
1:41 PM
1 :44 PM
1:46 PM
1:49 PM
1:51 PM
V.53PM
1:55 PM
2:07 PM
2:09 PM
2:11 PM
2:14 PM
2:17 PM
2:18 PM
2:20 PM
2:24 PM
2:38 PM
2:42 PM
2:44 PM
2:48 PM
2:58 PM
3:00 PM
3:17 PM
3:21 PM
3:24 PM
3:26 PM
3:32 PM
5:26 PM
5:28 PM
5:34 PM
5:36 PM
5:42 PM
5:46 PM
5:49 PM
5:51 PM
5:57 PM
6:01 PM
6:05 PM
6:10 PM
6:14 PM
6:17 PM
6:20 PM
5:02 AM
6:25 PM
6:31 PM
6:35 PM
;>mx£ PM^p^issifi
?^^;^^,Sr.' j*
Griffith Company
Bostick Co., J B
Interstate Asphalt
Griffith Company
Griffith Company
Griffith Company
Griffith Company
Bostick Co., J B
Interstate Asphalt
Griffith Company
Griffith Company
Griffith Company
Griffith Company
Bostick Co., J B
Silverado Constructors
Griffith Company
Griffith Company
Bostick Co., J B
Bostick Co., JB
Interstate Asphalt
Bostick Co., JB
Interstate Asphalt
Bostick Co., J B
Bostick Co., J B
T. B. S. Contractors
Bostick Co., J B
Bostick Co., J B
Silverado Constructors
Silverado Constructors
Bostick Co., J B
Silverado Constructors
Silverado Constructors
Silverado Constructors
Silverado Constructors
Silverado Constructors
Silverado Constructors
Silverado Constructors
Silverado Constructors
Silverado Constructors
Silverado Constructors
Silverado Constructors
Silverado Constructors
Silverado Constructors
Silverado Constructors
Silverado Constructors
Silverado Constructors
Silverado Constructors
Silverado Constructors
Silverado Constructors
1298
312501
15
230506
1001
2305
2305
11
3188
2475
102801
103202
201002
312505
221505
155404
201064
3419
29
21
44
18
9
12
25
312501
11
27
16
21
18
21
29
26
30
12
44
9
10
16
8
13
9
20
82
33
22
23
3
26.15
24.65
21.42
25.62
27.76
25.51
26
21.1
24.23
25.92
26.15
26.14
25.61
23.94
25.63
25.52
25.89
24.48
23.68
21.64
21.63
21.47
21.3
21.32
8
24.56
21.22
21.18
21.19
22.35
21.26
21.43
21.67
20.95
21.34
21.02
21.45
21.26
21.27
21.3
21.2
21.3
21.59
21.32
21.32
21.3
21.5
20.8
21.32
^V .^^^^^^CT^6wS^w3^^^ SISIBlfflBBffiilsss
1024 Type B 3/4" M.M. AR-4000
1010 HID AR-4000
1004 III C3 AR-4000
1024 Type B 3/4" M.M. AR-4000
1024 Type B 3/4" M.M. AR-4000
1024 Type B 3/4" M.M. AR-4000
1024 Type B 3/4" M.M. AR-4000
101 OHIO AR-4000
1004 III C3 AR-4000
1024 Type B 3/4" M.M. AR-4000
1024 Type B 3/4" M.M. AR-4000
1024 Type B 3/4" M.M. AR-4000
1024 Type B 3/4" M.M. AR-4000
1010 MID AR-4000
1066 Type B 3/8" AR-8000
1024 Type B 3/4" M.M. AR-4000
1024 Type B 3/4" M.M. AR-4000
1010 HID AR-4000
1010 HID AR-4000
1004 I II C3 AR-4000
101 OHIO AR-4000
1004 III C3 AR-4000
1010 HID AR-4000
101 OHIO AR-4000
1010 HID AR-4000
1010 HID AR-4000
101 OHIO AR-4000
1066 Type B 3/8" AR-8000
1066 Type B 3/8" AR-8000
1010 HID AR-4000
1024 Type B 3/4" M.M. AR-4000
1024 Type B 3/4" M.M. AR-4000
1024 Type B 3/4" M.M. AR-4000
1024 Type B 3/4" M.M. AR-4000
1024 Type B 3/4" M.M. AR-4000
1024 Type B 3/4" M.M. AR-4000
1024 Type B 3/4" M.M. AR-4000
1024 Type B 3/4" M.M. AR-4000
1024 Type B 3/4" M.M. AR-4000
1024 Type B 3/4" M.M. AR-4000
1024 Type B 3/4" M.M. AR-4000
1024 Type B 3/4" M.M. AR-4000
1024 Type B 3/4" M.M. AR-4000
1024 Type B 3/4" M.M. AR-4000
1024 Type B 3/4" M.M. AR-4000
1024 Type B 3/4" M.M. AR-4000
1024 Type B 3/4" M.M. AR-4000
1 024 Type B 3/4" M.M. AR-4000
1024 Type B 3/4" M.M. AR-4000
-------
LOAD-OUT DATA
FOR 7/28/98
" ^1^1
6:37 PM
6:40 PM
6:43 PM
6:47 PM
6:50 PM
7:09 PM
7:12 PM
7:15 PM
7:16 PM
7:1 9PM
7:26 PM
7:35 PM
7:37 PM
7:39 PM
Silverado Constructors
Silverado Constructors
Silverado Constructors
Silverado Constructors
Silverado Constructors
Silverado Constructors
Silverado Constructors
Silverado Constructors
Silverado Constructors
Silverado Constructors
Silverado Constructors
Silverado Constructors
Silverado Constructors
Silverado Constructors
\-A\V * ^iffit1 ^f^'
86
18
2
89
99
21
30
82
29
26
12
9
15
44
21.07
21.14
21.29
21.3
20.75
21.24
21.44
21.22
21.33
21.01
21.06
21.31
21.57
21.46
^^^!^|;B^M|^@83i3^
1024 Type B 3/4" M.M. AR-4000
1024 Type B 3/4" M.M. AR-4000
1024 Type B 3/4" M.M. AR-4000
1024 Type B 3/4" M.M. AR-4000
1024 Type B 3/4" M.M. AR-4000
1024 Type B 3/4" M.M. AR-4000
1024 Type B 3/4" M.M. AR-4000
1024 Type B 3/4" M.M. AR-4000
1024 Type B 3/4" M.M. AR-4000
1024 Type B 3/4" M.M. AR-4000
1024 Type B 3/4
" M.M. AR-4000
1024 Type B 3/4" M.M. AR-4000
1024 Type B 3/4" M.M. AR-4000
1024 Type B 3/4" M.M. AR-4000
-------
APPENDIX B.6
SILO NO. 2 LOAD-IN RECORDS USED IN SED EMISSION CALCULATIONS
-------
Asphalt Plant C Load-in Data for Silo #2 Used in Silo Exhaust Duct Emission Calculations
Client/Source:
Date
7/24/98
7/24/98
7/24/98
7/24/98
7/24/98
7/24/98
7/24/98
7/25/98
7/25/98
7/25/98
7/25/98
7/25/98
7/25/98
7/25/98
7/27/98
7/27/98
7/27/98
7/27/98
7/27/98
7/27/98
7/27/98
7/27/98
7/28/98
7/28/98
7/28/98
EPA Plant C
Hot Mix Asphalt
Test
Method
S-V-1-1
S-V-1-2
S-V-1-3
S-V-1-4
S-MM5-1
S-M315-1
S-M18-1
S-V-2-1
S-V-2-2
S-V-2-3
S-V-2-4
S-MM5-2
S-M315-2
S-M18-2
S-V-3-1
S-V-3-2
S-V-3-3
S-V-3-4
S-V-3-5
S-V-3-6
S-MM5-3
S-M18-3
S-MM5-4
S-MM5-5
S-M315-4
Run No.
Date:
Spreadsheet work:
Total Tons *
79.2
57.7
56.5
56.6
802.2
336.7
745.4
46.3
53.0
53.2
46.3
602.5
282.7
595.5
41.9
42.1
47.1
64.2
63.7
64.2
1079.5
472.4
881.0
709.4
402.4
Summary Runs 1-5
MA
Derek Hawkes
10
* Calculated from TPH Mix Rate Data taken from Production Records. Numbers in middle columns indicate sampling periods, Load
in tons are the calculated values used to estimate the total tons loaded per test period. Silofinb
-------
Asphalt Plant C Load-In Data for Silo #2 Used in Silo Exhaust Duct Emission Calculations
Client/Source:
Time
7:20
7:21
7:22
7:23
7:24
7:25
7:26
7:27
7:28
7:29
7:30
7:31
7:32
7:33
7:34
7:35
7:36
7:37
7:38
7:39
7:40
7:41
7:42
7:43
7:44
7:45
7:46
7:47
7:48
7:49
7:50
7:51
7:52
7:53
7:54
7:55
7:56
7:57
7:58
7:59
8:00
8:01
8:02
8:03
8:04
8:05
8:06
EPA Plant C
Hot Mix Asphalt
Load-out
Tons
21.45
21.34
21.39
20.10
21.04
21.19
21.12
21.27
21.12
21.17
Run No.
Date:
Spreadsheet work:
S-V-1 (1-4)
1
1
1
1
1
1
1
1
1
1
S-MM5-1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1-Load Out
7/24/1998
Derek Hawkes
S-M315-1
S-M18-1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
Load-In
Tons*
7.15
7.25
7.35
7.45
7.55
7.65
7.74
7.84
7.94
8.04
8.01
7.98
7.96
7.93
7.90
7.87
7.84
7.82
7.79
7.76
7.73
7.71
7.68
7.65
7.62
7.59
7.57
7.54
7.51
7.48
7.45
7.43
7.40
7.37
7.34
7.31
7.29
7.26
7.23
7.20
7.18
7.16
7.15
7.13
7.12
7.10
7.09
• rairuiatari from TPH Mix Rate Data taken frorn,, PjSJtufiliQn Records.. Numbers In middle columns Indicate sampling periods, Load
-------
Asphalt Plant C Load-In Data for Silo #2 Used in Silo Exhaust Duct Emission Calculations
7Z.
Client/Source: EPA Plant C
Hot Mix Asphalt
Time
8:07
8:08
8:09
8:55
8:56
8:57
8:58
8:59
9:00
9:01
9:02
9:03
9:04
9:05
9:06
9:07
9:08
9:09
9:18
9:19
9:20
9:21
9:22
9:23
9:24
9:25
9:26
9:27
9:28
9:29
9:30
9:31
9:32
9:33
9:34
9:35
9:36
9:37
9:38
9:39
9:40
9:41
9:42
9:43
9:44
9:45
9:46
Load-out
Tons
21.26
19.91
21.58
21.27
21.46
21.44
21.36
21.20
21.06
Run No. 1-Load Out
Date: 7/24/1998
Spreadsheet work: Derek Hawkes
S-V-1 (1-4)
2
2
2
2
2
2
2
2
2
2
3
3
3
3
3
3
3
3
3
3
S-MM5-1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
S-M315-1
S-M18-1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
Load-In
Tons*
7.07
7.06
7.05
5.94
5.91
5.88
5.85
5.81
5.78
5.78
5.77
5.77
5.77
5.76
5.76
5.76
5.75
5.75
5.72
5.71
5.71
5.70
5.70
5.70
5.69
5.69
5.69
5.68
5.68
5.67
5.67
5.67
5.66
5.66
5.66
5.65
5.65
5.65
5.65
5.65
5.65
5.65
5.65
5.65
5.65
5.65
5.65
* Calculated from TPH Mix Rate Data taken from Production Records. Numbers in middle columns indicate sampling periods, Load
in tons are the calculated values used to estimate the total tons loaded per test period. Silofinb
-------
Asphalt Plant C Load-In Data for Silo #2 Used in Silo Exhaust Duct Emission Calculations
"73
frr
Client/Source: EPA Plant C
Time
9:47
9:48
9:49
9:50
9:51
9:52
9:53
9:54
9:55
9:56
9:57
9:58
9:59
10:00
10:01
10:02
10:03
10:04
10:05
10:06
10:07
10:08
10:09
10:10
10:11
10:12,
10:13
10:14
10:15
10:16
10:17
11:41
11:42
11:43
11:44
11:45
11:46
11:47
11:48
11:49
11:50
11:51
11:52
11:53
11:54
11:55
11:56
Hot Mix Asphalt
Load-out
Tons
20.88
21.34
21.53
21.52
21.29
21.60
21.27
21.22
21.44
21.06
21.17
20.12
21.34
21.06
21.15
Run No. 1-Load Out
Date: 7/24/1998
Spreadsheet work: Derek Hawkes
S-V-1 (1-4)
4
4
4
4
4
4
4
4
4
4
S-MM5-1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
S-M315-1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
S-M18-1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
' 1
1
1
1
Load-In
Tons*
5.65
5.65
5.65
5.65
5.65
5.65
5.65
5.65
5.65
5.65
5.65
5.65
5.65
5.65
5.65
5.65
5.65
5.65
5.65
5.65
5.66
5.66
5.66
5.67
5.67
5.67
5.68
5.68
5.68
5.69
5.69
5.61
5.61 ,
5.61
5.61
5.61
5.61
5.61
5.61
5.61
5.61
5.61
5.61
5.61
5.61
5.61
5.61
..v, TDU Miv Rato nata taken frn.ni production R»coifla(,,JsluinJ)j80 in. middle columns indicate sampling periods, Load
-------
Asphalt Plant C Load-In Data for Silo #2 Used in Silo Exhaust Duct Emission Calculations
Client/Source:
Time
11:57
11:58
11:59
12:00
12:01
12:02
12:03
12:04
12:05
12:06
12:07
12:08
12:09
12:10
12:13
12:14
12:15
12:16
12:17
12:18
12:19
12:20
12:21
12:22
12:23
12:24
12:25
12:26
12:27
12:28
12:29
12:30
12:31
12:32
12:33
12:34
12:35
12:36
12:37
12:38
12:39
12:40
12:41
12:42
Total
EPA Plant C
Hot Mix Asphalt
Load-out
Tons
21.31
21.35
21.22
21.32
21.22
21.02
l_ 23.99
21.29
21.00
21.52
21.47
21.46
20.40
21.73
21.28
21.16
21.39
1495.56
Run No. 1-Load Out
Date: 7/24/1998
Spreadsheet work: Derek Hawkes
S-V-1 (1-4)
S-MM5-1
802.2
S-M315-1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
336.7
S-M18-1
745.4
Load-In
Tons*
5.61
5.61
5.61
5.61
5.61
5.61
5.61
5.61
5.61
5.61
5.61
5.61
5.61
5.61
5.61
5.61
5.61
5.61
5.61
5.61
5.61
5.61
5.61
5.61
5.61
5.61
5.61
5.61
5.61
5.61
5.61
5.61
5.61
5.62
5.62
5.62
5.62
5.62
5.62
5.62
5.62
5.62
5.62
5.62
* Calculated from TPH Mix Rate Data taken from Production Records. Numbers in middle columns indicate sampling periods, Load
in tons are the calculated values used to estimate the total tons loaded per test period. Silofmb
-------
Asphalt Plant C Load-In Data for Silo #2 Used in Silo Exhaust Duct Emission Calculations
T5"
* Calculated from TPH Mix Rate Data taken from Production Records. Numbers in middle columns indicate sampling periods, Load
Client/Source: EPA Plant C
Hot Mix Asphalt
Time
7:10
7:11
7:12
7:13
7:14
7:15
7:16
7:17
7:18
7:19
7:20
7:21
7:22
7:23
7:24
7:25
7:26
7:27
7:28
7:29
7:30
7:31
7:32
7:33
7:34
7:35
7:36
7:37
7:38
7:39
7:40
7:41
7:42
7:43
7:44
7:45
7:46
7:47
7:48
7:49
7:50
7:51
7:52
7:53
7:54
7:55
7:56
Load-out
Tons
22.00
23.87
21.21
22.00
24.43
22.00
23.24
20.64
21.26
Run No. 2-Load Out
Date: 7/25/1998
Spreadsheet work: Derek Hawkes
S-V-2 (1-4)
1
1
1
1
1
1
1
1
1
1
2
2
2
2
2
2
2
2
2
2
S-MM5-2
2
2
2
2
2
2
2
2
2
2
2
2
2
2
2
2
2
2
2
2
2
2
2
2
2
2
2
2
2
2
2
2
2
2
2
2
2
2
2
2
2
2
2
2
2
2
2
S-M315-2
S-M18-2
2
2
2
2
2
2
2
2
2
2
2
2
2
2
2
2
2
2
2
2
2
2
2
2
2
2
2
2
2
2
2
2
2
2
2
2
2
2
2
2
2
2
2
2
2
2
2
Load-In
Tons*
4.63
4.63
4.63
4.63
4.63
4.63
4.64
4.64
4.64
4.64
4.64
4.64
4.64
4.64
4.64
4.65
4.65
4.65
4.65
4.65
4.65
4.65
4.65
4.65
4.66
4.66
4.66
4.66
4.66
4.66
4.66
4.72
4.78
4.84
4.90
4.96
5.02
5.09
5.15
5.21
5.27
5.33
5.39
5.45
5.51
5.57
5.63
-------
Asphalt Plant C Load-In Data for Silo #2 Used in Silo Exhaust Duct Emission Calculations
Client/Source:
Time
7:57
7:58
7:59
8:00
8:01
8:02
8:03
8:04
8:05
8:06
8:07
8:08
8:09
8:40
8:41
8:42
8:43
8:44
8:45
8:46
8:47
8:48
8:49
8:50
8:51
8:52
8:53
8:54
8:55
8:56
8:57
8:58
8:59
9:00
9:01
9:02
9:03
9:04
9:05
9:06
9:07
9:08
9:09
9:10
9:11
9:12
9:13
EPA Plant C
Hot Mix Asphalt
Load-out
Tons
21.26
21.05
22.00
24.47
21.18
22.00
23.80
45.67
Run No.
Date:
Spreadsheet work:
S-V-2(1-4)
3
3
3
3
3
3
3
3
3
3
4
4
4
4
S-MM5-2
2
2
2
2
2
2
2
2
2
2
2
2
2
2
2
2
2
2
2
2
2
2
2
2
2
2
2
2
2
2
2
2
2
2
2
2
2
2
2
2
2
2
2
2
2
2
2
2-Load Out
7/25/1998
Derek Hawkes
S-M315-2
S-M18-2
2
2
2
2
2
2
2
2
2
2
2
2
2
2
2
2
2
2
2
2
2
2
2
2
2
2
2
2
2
2
2
2
2
2
2
2
2
2
2
2
2
2
2
Load-In
Tons*
5.69
5.75
5.81
5.87
5.93
5.99
6.05
6.11
6.18
6.24
6.30
6.36
6.42
5.83
5.81
5.77
5.73
5.69
5.65
5.61
5.57
5.53
5.50
5.46
5.42
5.38
5.34
5.30
5.26
5.22
5.18
5.14
5.10
5.06
5.02
4.98
4.94
4.91
4.87
4.83
4.79
4.75
4.71
4.67
4.63
4.63
4.63
* Calculated from TPH Mix Rate Data taken from Production Records. Numbers In middle columns indicate sampling periods, Load
in tons are the r.alrulateri values nseri to estimate the total tons loarlnri ner test neriori Silofinb
-------
Asphalt Plant C Load-In Data for Silo #2 Used in Silo Exhaust Duct Emission Calculations
77
Client/Source: EPA Plant C
Time
9:14
9:15
9:16
9:17
9:18
9:19
9:30
9:31
9:32
9:33
9:34
9:35
9:36
9:37
9:38
9:39
9:40
9:41
9:42
9:43
9:44
9:45
9:46
9:47
9:48
9:49
9:50
9:51
9:52
9:53
10:15
10:16
10:17
10:18
10:19
10:20
10:21
10:22
10:23
10:24
10:25
10:26
10:27
10:28
10:29
10:30
10:31
Hot Mix Asphalt
Load-out
Tons
20.87
21.02
12.00
20.94
8.00
21.10
23.87
15.03
24.58
21.17
23.54
22.00
24.06
Run No. 2-Load Out
Date: 7/25/1998
Spreadsheet work: Derek Hawkes
S-V-2 (1-4)
4
4
4
4
4
4
S-MM5-2
2
2
2
2
2
2
2
2
2
2
2
2
2
2
2
2
2
2
2
2
2
2
2
2
2
2
S-M315-2
2
2
2
2
2
2
2
2
2
2
2
2
2
2
2
2
2
S-M18-2
2
2
2
2
2
2
2
2
2
2
2
2
2
2
2
2
2
2
2
2
2
2
2
2
2
2
2
2
2
2
Load-In
Tons*
4.63
4.63
4.63
4.63
4.63
4.63
4.62
4.62
4.62
4.62
4.62
4.62
4.62
4.62
4.62
4.62
4.62
4.62
4.62
4.61
4.61
4.60
4.60
4.59
4.59
4.58
4.58
4.58
4.57
4.57
4.55
4.56
4.58
4.60
4.61
4.63
4.65
4.66
4.68
4.69
4.71
4.73
4.74
4.76
4.78
4.79
4.81
,nm TDU Miv Rate
Production Records. Nu^t^rs in middle columns indicate sampling periods, Load
-------
Asphalt Plant C Load-In Data for Silo #2 Used in Silo Exhaust Duct Emission Calculations
Client/Source:
Time
10:32
10:33
10:34
10:35
10:36
10:37
10:38
10:39
10:40
10:41
10:42
10:43
10:44. .
10:47
10:48
10:49
10:50
10:51
10:52
10:53
10:54
10:55
10:56
10:57
10:58
10:59
11:00
11:01
11:02
11:03
11:04
11:05
11:06
11:07
11:08
11:09
11:10
11:11
11:12
11:13
11:14
11:15
11:16
Total
EPA Plant C
Hot Mix Asphalt
Load-out
Tons
20.80
20.87
20.91
20.91
21.07
21.13
1154.48
Run No.
Date:
Spreadsheet work:
S-V-2(1-4)
S-MM5-2
602.5
2-Load Out
7/25/1998
Derek Hawkes
*
S-M315-2
2
2
2
2
2
2
2
2
2
2
2
2
2
2
2
2
2
2
2
2
2
2
2
2
2
2
2
2
2
2
2
2
2
2
2
2
2
2
2
2
2
2
2
282.7
S-M18-2
595.5
Load-In
Tons*
4.83
4.84
4.86
4.87
4.89
4.91
4.92
4.94
4.96
4.97
4.96
4.95
4.94
4.91
4.90
4.89
4.88
4.87
4.86
4.86
4.85
4.84
4.83
4.82
4.81
4.80
4.79
4.78
4.77
4.76
4.75
4.74
4.73
4.72
4.71
4.70
4.69
4.49
4.30
4.10
3.91
3.71
3.52
Calculated from TPH Mix Rate Data taken from Production Records. Numbers in middle columns indicate sampling periods, Load
-------
Asphalt Plant C Load-In Data for Silo #2 Used in Silo Exhaust Duct Emission Calculations
Client/Source:
Time
8:04
8:05
8:06
8:07
8:08
8:09
8.10
8:11
8:12
8:13
8:14
8:15
8:16
8:17
8:18
8:19
8:20
8:21
8:22
8:23
8:24
8:25
8:26
8:27
8:28
8:29
8:30
8:31
8:32
8:33
8:34
8:35
8:36
8:37
8:38
8:39
8:40
8:41
8:42
8:43
8:44
8:45
8:46
8:47
8:48
8:49
8:50
EPA Plant C
Hot Mix Asphalt
Load-out
Tons
12.70
13.84
14.00
21.40
12.00
12.25
25.76
13.00
12.56
11.56
12.48
21.38
24.23
25.71
13.03
13.13
12.80
13.04
13.00
12.96
21.12
Run No.
Date:
Spreadsheet work:
S-V-3 (1-4)
1
1
1
1
1
2
2
2
2
2
S-MM5-3
3
3
3
3
3
3
3
3
3
3
3
3
3
3
3
3
3
3
3
3
3
3
3
3
3
3
3
3
3
3
3
3
3
3
3
3
3
3
3
3
3
3
3
3
3
3
3
3-Load Out
7/27/1998
Derek Hawkes
S-M315-3
S-M18-3
Load-In
Tons*
8.37
8.37
8.37
8.37
8.37
8.37
8.37
8.37
8.38
8.38
8.38
8.38
8.38
8.38
8.38
8.38
8.38
8.38
8.38
8.39
8.39
8.39
8.39
8.39
8.39
8.39
8.39
8.39
8.40
8.40
8.43
8.45
8.48
8.51
8.54
8.57
8.60
8.62
8.65
8.68
8.71
8.74
8.77
8.79
8.82
8.85
8.88
re in miririio columns indicate sampling periods, Load
-------
Asphalt Plant C Load-In Data for Silo #2 Used in Silo Exhaust Duct Emission Calculations
Client/Source:
Time
8:51
8:52
8:53
8:54
8:55
8:56
8:57
8:58
8:59
9:00
9:01
9:02
9:03
9:25
9:26
9:27
9:28
9:29
9:30
9:31
9:32
9:33
9:34
9:35
9:38
9:39
9:40
9:41
9:42
9:48
9:49
9:50
9:51
9:52
9:53
9:54
9:55
9:56
9:57
9:58
9:59
10:00
10:01
10:02
10:03
10:04
10:05
EPA Plant C
Hot Mix Asphalt
Load-out
Tons
21.33
13.00
13.13
11.59
12.86
21.31
20.44
13.14
11.47
13.00
26.06
11.05
12.77
12.77
21.36
13.00
12.71
13.00
14.74
21.49
12.05
12
12.65
13.23
13.12
13.27
21.26
21.07
13.00
13.08
12.86
Run No.
Date:
Spreadsheet work:
S-V-3 (1-4)
3
3
3
3
3
4
4
4
4
4
4
4
S-MM5-3
3
3
3
3
3
3
3
3
3
3
3
3
3
3
3
3
3
3
3
3
3
3
3
3
3
3
3
3
3
3
3
3-Load Out
7/27/1998
Derek Hawkes
S-M315-3
S-M18-3
Load-In
Tons*
8.91
8.94
8.96
8.99
9.02
9.05
9.08
9.09
9.11
9.13
9.15
9.17
9.18
9.57
9.59
9.61
9.60
9.58
9.57
9.55
9.54
9.52
9.51
9.49
9.45
9.43
9.42
9.40
9.39
9.30
9.28
9.27
9.25
9.24
9.22
9.21
9.19
9.18
9.16
9.16
9.16
9.16
9.15
9.15
9.15
9.15
9.15
• Calculated from TPH Mix Rate Data taken from Production Records. Numbers in middle columns indicate sampling periods, Load
in tons are the calculated values used to estimate the total tons loaded per test period. Silofinb
-------
Asphalt Plant C Load-In Data for Silo #2 Used in Silo Exhaust Duct Emission Calculations
Calculated frt
Client/Source: EPA Plant C
Hot Mix Asphalt
Time
10:06
10:07
10:08
10:09
10:10
10:11
10:12
10:13
10:14
10:15
10:16
10:17
10:18
10:19
10:20
10:21
10:22
10:23
10:24
10:25
10:26
10:27
10:28
10:29
10:30
10:31
10:32
10:33
10:34
10:35
10:36
10:37
10:38
10:39
10:40
10:41
10:42
10:43
10:44
10:45
10:46
10:47
10:48
10:49
10:50
10:51
10:52
Load-out
Tons
12.92
24.42
34.33
25.93
13.00
12.22
1261
12.17
13.00
12.86
12.79
11.73
21.25
12.82
12.90
13.00
13.14
20.98
8.95
13.00
13.10
13.00
12.76
21.21
21.44
Run No. 3-Load Out
Date: 7/27/1998
Spreadsheet work: Derek Hawkes
S-V-3 (1-4)
5
5
5
5
5
5
5
6
6
6
6
6
6
6
S-MM5-3
3
3
3
3
3
3
3
3
3
3
3
3
3
3
3
3
3
3
3
3
3
3
3
3
3
3
3
3
3
3
3
3
3
3
3
3
3
3
3
3
3
3
3
S-M315-3
S-M18-3
3
3
3
3
3
3
3
3
3
3
3
3
3
3
3
3
3
3
3
3
3
3
3
3
3
3
3
3
3
3
Load-In
Tons'
9.14
9.14
9.14
9.14
9.14
9.13
9.13
9.13
9.13
9.12
9.12
9.12
9.12
9.12
9.11
9.11
9.11
9.11
9.10
9.10
9.10
9.10
9.10
9.11
9.12
9.12
9.13
9.14
9.14
9.15
9.16
9.16
9.17
9.18
9.18
9.19
9.20
9.20
9.21
9.21
9.22
9.23
9.23
9.24
9.25
9.25
9.26
'
>m TPH Mix Rate Data taken from Production Records. Numbers in middle columns Indicate sampling periods, Load
-------
Asphalt Plant C Load-In Data for Silo #2 Used in Silo Exhaust Duct Emission Calculations
Client/Source:
Time
11:40
11:41
11:42
11:43
11:44
11:45
11:46
11:47
11:48
11:49
11:50
11:51
11:52
11:53
11:54
12:43
12:44
12:45
12:46
12:47
Total
EPA Plant C
Hot Mix Asphalt
Load-out
Tons
15.67
13.00
13.10
12.00
12.49
13.00
12.96
13.00
12.46
24.81
12.00
2378.16
Run No.
Date:
Spreadsheet work:
S-V-3(1-4)
S-MM5-3
1079.5
3-Load Out
7/27/1998
Derek Hawkes
S-M315-3
0.0
S-M18-3
3
3
3
3
3
3
3
3
3
3
3
3
3
3
3
3
3
3
3
3
472.4
Load-In
Tons*
9.92
9.95
9.98
10.01
10.04
10.07
10.09
10.12
10.15
10.18
10.21
10.24
10.26
10.29
10.32
9.10
9.10
9.10
9.10
9.10
* Calculated from TPH Mix Rate Data taken from Production Records. Numbers in middle columns indicate sampling periods, Load
in tons are the calculated values used to estimate the total tons loaded per test period. Silofinb
-------
Asphalt Plant C Load-In Data for Silo #2 Used in Silo Exhaust Duct Emission Calculations
Client/Source:
Time
6:49
6:49
6:50
6:51
6:52
6:53
6:54
6:55
6:56
6:57
6:58
6:59
7:00
7:01-
7:02
7:03
7:04
7:05
7:06
7:07
7:08
7:09
7:10
7:11
7:12
7:13
7:14
7:15
7:16
7:17
7:18
8:10
8:11
8:12
8:13
8:14
8:15
8:16
8:17
8:18
8:19
8:20
8:21
8:22
8:23
8:24
8:25
EPA Plant C
Hot Mix Asphalt
Load-out
Tons
Run No.
Date:
4&5-Load Out
7/28/1998
Spreadsheet work: Derek Hawkes
S-MM5-4
S-MM5-5
S-M315-4
4
4
4
4
4
4
4
4
4
4
4
4
4
4
4
4
4
4
4
4
4
4
4
4
4
4
4
4
4
4
4
4
4
4
4
4
4
4
4
4
4
4
4
4
4
4
4
Load-In
Tons*
5.29
5.34
5.38
5.42
5.47
5.51
5.56
5.60
5.64
5.69
5.73
5.78
5.82
5.87
5.91
5.95
6.00
6.04
6.09
6.13
6.18
6.22
6.26
6.31
6.35
6.40
6.44
6.49
6.47
6.45
6.44
6.79
6.82
6.85
6.88
6.91
6.94
6.98
7.01
7.05
7.08
7.11
7.15
7.18
7.22
7.25
7.29
tort from TPH Mix Rate Data taken from Production Records. Numbers In middle columns Indicate sampling periods, toad
-------
Asphalt Plant C Load-In Data for Silo #2 Used in Silo Exhaust Duct Emission Calculations
Client/Source:
Time
8:26
8:27
8:28
8:29
8:30
8:31
8:32
8:33
8:34
8:35
8:36
8:37
8:38
8:39
9:13
9:14
9:15
9:16
9:17
9:18
9:19
9:20
9:21
9:22
9:23
9:24
9:25
9:26
9:27
9:28
9:29
9:30
9:31
9:32
9:33
9:34
9:35
9:36
9:37
10:26
10:27
10:28
10:29
10:30
10:31
10:32
10:33
EPA Plant C
Hot Mix Asphalt
Load-out
Tons
Run No. 4&5-Load Out
Date: 7/28/1998
Spreadsheet work: Derek Hawkes
S-MM5-4
4
4
4
4
4
4
4
4
4
4
4
4
4
4
4
4
4
4
4
4
4
4
4
4
4
4
4
4
4
4
4
4
4
S-MM5-5
S-M315-4
4
4
4
4
4
4
4
4
4
4
4
4
4
4
Load-In
Tons*
7.32
7.36
7.39
7.42
7.46
7.49
7.53
7.56
7.60
7.63
7.67
7.70
7.74
7.77
7.92
7.92
7.92
7.89
7.86
7.83
7.81
7.78
7.75
7.73
7.70
7.67
7.64
7.62
7.59
7.56
7.54
7.51
7.48
7.46
7.43
7.50
7.56
7.63
7.70
7.18
7.19
7.21
7.23
7.25
7.26
7.28
7.30
* Calculated from TPH Mix Rate Data taken from Production Records. Numbers in middle columns indicate sampling periods, Load
in tons are the calculated values used to estimate the total tons loaded per test period. Silofinb
-------
Asphalt Plant C Load-In Data for Silo #2 Used in Silo Exhaust Duct Emission Calculations
Client/Source: EPA Plant C
Time
10:34
10:35
10:36
10:37
10:38
10:39
10:40
10:41
10:42
10:43
10:44
10:45
10:46
10:47
10:48
10:49
10:50
10:51
10:52
10:53
10:54
10:55
10:56
10:57
10:58
10:59
11:00
11:39
11:40
11:41
11:42
11:43
11:44
11:45
11:46
11:47
11:48
12:33
12:34
12:35
12:36
12:37
12:38
12:39
12:40
12:41
' 12:42
Hot Mix Asphalt
Load-out
Tons
Run No. 4&5-Load Out
Date: 7/28/1998
Spreadsheet work: Derek Hawkes
S-MM5-4
4
4
4
4
4
4
4
4
4
4
4
4
4
4 .
4
4
4
4
4
4
4
4
4
4
4
4
4
4
4
4
4
4
4
4
4
4
4
4
4
4
4
4
4
4
4
4
4
S-MM5-5
S-M315-4
Load-In
Tons*
7.32
7.33
7.35
7.37
7.39
7.41
7.42
7.44
7.46
7.48
7.49
7.51
7.51
7.51
7.51
7.51
7.50
7.50
7.50
7.50
7.50
7.50
7.50
7.49
7.49
7.49
7.49
7.63
7.63
7.64
7.65
7.65
7.66
7.67
7.66
7.66
7.66
7.48
7.47
7.46
7.45
7.44
7.43
7.42
7.40
7.39
7.38
rnm TPH Mix Rate Data taken from Projyction Records. Numbers in middle columns Indicate sampling periods, Load
-------
Asphalt Plant C Load-In Data for Silo #2 Used in Silo Exhaust Duct Emission Calculations
%£»
Client/Source:
Time
12:43
12:44
12:45
12:46
12:47
12:48
12:49
12:50
12:51
12:52
12:53
12:54
12:55
12:56
12:57
12:58
12:59
13:00
13:01
13:02
13:03
13:04
13:05
13:06
13:07
13:08
13:09
13:10
13:11
13:12
13:13
13:14
13:15
13:16
13:17
13:18
13:19
13:20
13:21
13:22
13:58
13:59
14:00
14:01
14:02
14:03
14:04
EPA Plant C
Hot Mix Asphalt
Load-out
Tons
Run No.
Date:
Spreadsheet work.
S-MM5-4
4
4
4
4
4
4
4
4
4
4
4
4
4
4
4
4
4
4
4
4
4
4
4
4
4
4
4
4
4
4
4
4
4
4
4
4
4
4
4
4
S-MM5-5
5
5
5
5
5
5
5
4&5-Load Out
7/28/1998
Derek Hawkes
S-M315-4
Load-In
Tons*
7.37
7.36
7.35
7.33
7.30
7.28
7.26
7.24
7.22
7.19
7.17
7.15
7.13
7.11
7.08
7.06
7.04
7.02
7.00
5.61
6.97
6.95
6.93
6.91
6.89
6.86
6.84
6.82
6.80
6.77
6.75
6.73
6.71
6.69
6.72
6.76
6.79
6.83
6.87
6.90
7.90
7.91
7.93
7.94
7.95
7.96
7.97
- calculated from TPH Mix Rate Data taken from Production Records. Numbers in middle columns indicate sampling periods, Load
in tons are the calculated values used to estimate the total tons loaded nar test neriod Sitofinb
-------
Asphalt Plant C Load-In Data for Silo #2 Used in Silo Exhaust Duct Emission Calculations
Client/Source:
Time
14:05
14:06
14:07
14:08
14:09
14:10
14:11
14:12
14:13
14:14
14:15
14:16
14:17
14:18
14:19
14:20
14:21
14:22
14:23
14:24
14:25
14:26
14:27
14:28
14:29
14:30
14:31
14:32
18:13
18:14
18:15
18:16
18:17
18:18
18:19
18:20
18:21
18:22
18:23
18:24
18:25
18:26
18:27
18:28 _,
18:29
18:30
18:31
EPA Plant C
Hot Mix Asphalt
Load-out
Tons
Run No.
Date:
Spreadsheet work:
S-MM5-4
S-MM5-5
5
5
5
5
5
5
5
5
5
5
5
5
5
5
5
5
5
5
5
5
5
5
5
5
5
5
5
5
5
5
5
5
5
5
5
5
5
5
5
5
5
5
5
5
5
5
5
4&5-Load Out
7/28/1998
Derek Hawkes
S-M315-4
Load-In
Tons*
7.98
7.99
8.01
8.02
8.03
8.04
8.05
8.06
8.07
8.09
8.10
8.11
8.09
8.06
8.04
8.02
8.00
7.98
7.95
7.93
7.91
7.89
7.87
7.85
7.82
7.80
7.78
7.76
2.91
2.89
2.98
3.07
3.15
3.24
3.33
3.41
3.50
3.59
3.67
3.76
3.85
3.94
4.02
4.11
4.20
4.28
4.37
i *rnm TPH Mix Rate Data taken from Production Re,c.p.rd.s. Numbers in middle columns Indicate sampling periods, Load
-------
Asphalt Plant C Load-In Data for Silo #2 Used in Silo Exhaust Duct Emission Calculations
}&
y&
Run No. 4&5-Load Out
Client/Source: EPA Plant C
Time
18:32
18:33
18:34
18:35
18:36
18:37
18:40
18:41
18:42
18:43
18:44
18:45
18:46
18:47
18:48
18:49
18:50
18:51
18:52
18:53
18:54
18:55
18:56
18:57
18:58
18:59
19:00
19:01
19:02
19:03
19:04
19.05
19:06
19:07
19:08
19:09
19:10
19:11
19:12
19:13
19:14
19:15
19:16
19:17
19:18
19:19
19:20
Date: 7/28/1998
Hot Mix Asphalt Spreadsheet work: Derek Hawkes
Load-out
Tons
S-MM5-4
S-MM5-5
5
5
5
5
5
5
5
5
5
5
5
5
5
5
5
5
5
5
5
5
5
5
5
5
5
5
5
5
5
5
5
5
5
5
5
5
5
5
5
5
5
5
5
5
5
5
5
S-M315-4
Load-In
Tons*
4.46
4.54
4.63
4.72
4.81
4.89
5.15
5.24
5.33
5.41
5.50
5.50
5.50
5.50
5.50
5.51
5.51
5.51
5.51
5.51
5.51
5.51
5.51
5.51
5.51
5.51
5.50
5.50
5.50
5.50
5.50
5.50
5.50
5.49
5.49
5.49
5.49
5.49
5.49
5.48
5.48
5.48
5.48
5.48
5.48
5.48
5.48
Calculated from TPH Mix Rate Data taken from Production Records. Numbers in middle columns indicate sampling periods, Load
-------
Asphalt Plant C Load-In Data for Silo #2 Used in Silo Exhaust Duct Emission Calculations
Client/Source:
Time
19:21
19:22
19:23
19:24
19:25
19:26
19:27
19:28
19:29
19:30
19:31
19:32
19:33
19:34
19:35
19:36
19:37
19:38
19:39
19:40
Total
EPA Plant C
Hot Mix Asphalt
Load-out
Tons
Run No.
Date:
Spreadsheet work:
S-MM5-4
881.0
S-MM5-5
5
5
5
5
5
5
5
5
5
5
5
5
5
5
5
5
5
5
5
5
709.4
4&5-Load Out
7/28/1998
Derek Hawkes
S-M315-4
402.4
Load-In
Tons*
5.48
5.48
5.48
5.48
5.48
5.48
5.48
5.48
5.48
5.48
5.48
5.48
5.48
5.48
5.48
5.48
5.48
5.48
5.48
5.48
* Calculated from TPH ML* Raje Djta taken from Prod.uctj°n
- Numbers in middle columns Indicate sampling periods, Load
-------
APPENDIX B.7
ASPHALT TEMPERATURES AT LOAD-OUT, 7/24/98 THROUGH 7/28/98
-------
ASPHALT PLANT C IN LOS ANGELES, CA
Measurements recorded by Jessica Swift
ASPHALT TEMPERATURES AT LOAD-OUT
Date
7/24/98
7/24/98
7/24/98
7/24/98
7/24/98
7/24/98
7/24/98
7/24/98
7/24/98
Average
Day 1
Time
7:25
7.31
7:36
11:12
11:15
11:20
13:16
13:20
13:26
Truck*
89
99
92
88
89
12
9
13
16
Temp. T
308
310
311
264
312
311
314
308
312
305.6
Temperature, F
Temp. B
320
315
309
310
318
312
320
310
315
314.3
Temp. B adj.
327
322
316
317
325
319
327
317
322
321.3
Day1
Comments
Temp. B adj. used in report
7/25/98
7/25/98
7/25/98
7/25/98
7/25/98
7/25/98
7/25/98
7/25/98
7/25/98
Day 2
Time
7:33
7;36
7.39
9'32
935
9:37
11:48
11.56
12.00
27
T-3
23
21
8
9
16
18
27
Temperature, F
Temp. T
313
332
333
285
306
314
320
307
292
Temp B
310
325
322
282
305
313
320
310
292
308.8
Temp B adj.
317
332
329
289
312
320
327
317
299
Day 2
Comments
Temp. B adj used in report
71 7/98
7/ 7/98
7/ 7/98
7/ 7/98
71 7/98
71 7/98
71 7/98
71 7/98
Day 3
8.06
8-11
9.41
9:45
9:55
12.45
12:47
12:51
16
CA1138
27
' f-1
2305-2
CA20119
0-8
CA21784
268
278
285
284
294
283
301
300
Temperature, F
265
290
270
285
300
285
302
292
Temp. B ad
272
297
277
292
307
292
309
299
Day 3
Temp. B adj. used in report
7/28/98
7/28/98
Day 4
7:15
7 30
Truck #
na
na
Temperature, F
212
212
212
Temp. B
205
205
Temp B adj.
7
7
7.3
Day 4
Instruments Calibrated in boiling water
Instruments Calibrated in boiling water
Notes:
1. Temp T was taken with a PES thermocouple (TC).
2. Temp B was taken with a CAAP dial thermometer (dial).
3. Both instruments were inserted into the hot asphalt in the bed of the truck just after load-out
4. The dial was usually inserted first In some cases the dial reads higher than the TC. In these cases the TC was probably pulled out before reaching temperature.
5. Both instruments were calibrated on 7/28/98 in boiling water. Temp B adj. Represents adjusted values for Temp B.
asphtemp.XLS,Asphalt Temp
-------
APPENDIX B.8
MASS CHANGE RESULTS FROM ASTM TESTS
PERFORMED ON ASPHALT CEMENT SAMPLES
-------
ASPHALT PLANT C - RESULTS FROM ADVANCED ASPHALT TECHNOLOGIES
Asphalt Binder Samples - ASTM Analysis Results for Asphalt Plant C in Los Angeles, CA j
Two analyses were performed at three temperatures (300,325,and 350 Degrees F)
1. ASTM D1754-94 - Effects of Heat and Air on Asphalt Materials (TFOT)
2. ASTM D2872-88 - Effects of Heat and Air on a Moving Film of Asphalt (RTFOT)
Sample
Date
9/17/97
5/14/98
6/5/98
6/21/98
7/14/98
Sample
Time
nav
nav
nav
nav
nav
Day
Number
Pretest
Pretest
Pretest
Pretest
Pretest
Sample
ID
A1
A2
A3
A4
A5
Oven Temp. 325 F
*
TFOT
-0.030
-0.222
-0.178
-0.214
-0.216
RTFOT
-0.094
-0.417
-0.366
-0.398
-0.383
Oven Temp. 300 F
TFOT*
na
na
na
na
na
RTFOT*
na
na
na
na
na
Oven Temp. 350 F
TFOT*"
-0.097
-0.477
na
na
na
RTFOT
-0.185
-0.684
na
na
na
Sample
Date
7/24/98
7/24/98
7/24/98
Sample
Time
7:21 AM
11:05 AM
12:54 PM
Day
Number
Day 1
Day 1
Day 1
Sample
ID
AC1B
AC1M
AC1E
Average
Oven Temp. 325 F
TFOT
-0.175
-0.178
-0.196
-0.183
RTFOT
-0.347
-0.369
-0.370
-0.362
Oven Temp. 300 F
TFOT
na
-0.100
na
-0.100
RTFOT
na
-0.216
na
-0.216
Oven Temp. 350 F
TFOT
na
na
na
na
RTFOT
na
-0.686
na
-0.686
Sample
Date
7/25/98
7/25/98
7/25/98
Sample
Time
7:16 AM
9:18 AM
11:18AM
Day
Number
Day 2
day 2
Day 2
Sample
ID
AC2B
AC2M
AC2E
Average
Oven Temp. 325 F
TFOT
-0.182
-0.173
-0.186
-0.180
RTFOT
-0.313
-0.311
-0.341
-0.322
Oven Temp. 300 F
TFOT
na
0.090
na
-0.090
RTFOT
na
-0.200
na
-0.200
Oven Temp. 350 F
TFOT
na
na
na
na
RTFOT
na
-0.611
na
-0.611
Sample
Date
7/27/98
7/27/98
7/27/98
Sample
Time
7:28 AM
9:29 AM
12:24 PM
Day
Number
Day 3
Day3
Day 3
Sample
ID
AC3B
AC3M
AC3E
Average
Oven Temp. 325 F
TFOT
-0.146
-0.166
-0.150
-0.154
RTFOT
-0.301
-0.286
-0.264
-0.284
Oven Temp. 300 F
TFOT
na
na
na
na
RTFOT
na
-0.142
na
-0.142
Oven Temp. 350 F
TFOT
na
na
na
na
RTFOT
na
-0.498
na
-0.498
Sample
Date
7/28/98
7/28/98
7/28/98
7/28/98
Sample
Time
7:41 AM
9:17 AM
1:51 PM
7:43 PM
Day
Number
Day 4
Day 4
Day 4
Day 4
Sample
ID
AC4B
AC5B
AC6B
AC6E
Average
Oven Temp. 325 F
TFOT
-0.141
-0.157
-0.095
-0.237
-0.158
RTFOT
-0.361
-0.292
-0.322
-0.408
-0.346
Oven Temp. 300 F
TFOT
na
na
na
na
na
RTFOT
na
-0.171
na
na
-0.171
Oven Temp. 350 F
TFOT
na
na
na
na
na
RTFOT
na
-0.510
na
na
-0.510
| Overall Average
Oven Temp. 325 F
TFOT
-0.169
RTFOT
-0.328
Oven Temp. 300 F
TFOT
-0.095
RTFOT
-0.182
Oven Temp. 350 F
TFOT
-0.477
RTFOT
-0.576
nav = not available
na = not applicable, i.e., analysis was not performed
'fr-
et
-------
ADVANCED ASPHALT TECHNOLOGIES
LABORATORY AND TECHNICAL SERVICES
TEST REPORT
Test Report No.:
Report Date:
03840001.DOC
05/27/98
X| Original
I I Amended
page I of I
Client:
Pacific Environmental Services, Inc.
560 herndon Parkway, Suite 200
Herndon Virginia 20170-5240
Report Distribution: Mr. Frank Phoenix
Sample No.: AC496 & AC497
Project No.: WO#384
Description : Mass Loss Study for Pacific
Environmental
Date Received: 5/20/98
Sample Description: WHH^HHB" - AAT# AC496
Technical Responsibility
Name William Pennington
Title: Binder Team Leader
Signature: t^U^4 Q^^^
Date: ^7Z7/^ "
Technical Contact
Name: Kevin J. Knechtel
Title: Laboratory Manager j A }
Signature: <&_ $ . ft^f?
Date: ' /'*r/^7/-) £
Comments: - this a ifrue record of test results obtained by Advanced Asphalt Tedhnol&gies, L.P. in
accordance with the test methods and procedures stipulated by AASHTO/ASTM.
Test Results
Test
Mass Change, using the Thin Film Oven Test
(TFOT) at 325°F
Mass Change, using the Rolling Thin Film Oven Test
(RTFOT) at 325°F
Mass Change, using the Thin Film Oven Test
(TFOT) at 350°F
Mass Change, using the Rolling Thin Film Oven Test
(RTFOT) at 350°F
Method
Test Result
ASTM D 1754
ASTM D 2872
*ASTM D 1754
*ASTM D 2872
AC496 /
AAA
-0.222
-0.417
-0.477
-0.684
AC497 / All
American
-0.030
-0.094
-0.097
-0.185
*Note: Temperature of 350°F deviates from ASTM D1754 and ASTM D2872 standard test inethods. An A
13C thermometer was calibrated at 350°F, marked and used to conduct these non-sta idard tests. Th
was approved by Mr. Frank Phoenix.
TM
ftl
Advanced Asphalt
Technologies, LP
108 POWERS COURT, SUITE 100
STERLING, VA 20166-9321
PH (800) 395 6686
PH (703) 444 4200
FX (703)4444368
-------
ADVANCED ASPHALT TECHNOLOGIES
LABORATORY AND TECHNICAL SERVICES
TEST REPORT
Test Report No.:
Report Date:
03840003.DOC
07/20/98
_Xj Original
J Amended
page lofl
Client:
Pacific Environmental Services, Inc.
560 Herndon Parkway, Suite 200
Herndon Virginia 20170-5240
Report Distribution: Mr. Frank Phoenix
Sample No.: AC508, AC517, & AC564
Project No.: WCW384
Description: Mass Loss Study for Pacific
Environmental
Date Received: 6/12/98, 6/29/98, and
7/16/98
Sample Description: *JHBBMMBB^||t 6/5/98" - AAT# AC508
Technical Responsibility
Name William Pennington
Title : Binder Team Leader
Signature: ^c^^ 6£+^Y&tr-
Date: T/Wf?
Technical Contact
Name: Kevin J. Knechtel
Title: Laboratory Manager A
Signature: <,^ ft 9&M
Date: ' {/ 7/teht
Comments: '- This a true record of test results obtained by Advanced Asphalt Technologies, L.P. in
accordance with the test methods and procedures stipulated by AASHTO/ASTM.
Test Results
Test
Mass Change, using the
Thin Film Oven Test
(TFOT) at 325°F
Mass Change, using the
Rolling Thin Film Oven Test
(RTFOT) at 325°F
Method
ASTMD 1754
ASTM D 2872
Test Result 'A
AC508
All-American
Asphalt, Sampled-
6/5/98
-0.178
-0.366
^
AC517
All-American
Asphalt, Sampled-
6/21/98
-0.214
-0.398
AM
AC564
All-American
Asphalt, Sampled-
7/14/98
-0.216
-0.383
ftr
* flte oU^e °/
fr
Advanced Asphalt
Technologies, LP
108 POWERS COURT, SUITE 100
STERLING, VA 20166-9321
PH (800)3956686
PH (703)4444200
FX (703) 444 4368
-------
ADVANCED^SPHALT TECHNOLOGIES
LABORATORY AND TECHNICAL SERVICES
TEST REPORT
Test Report No.:
Report Date:
03840004.DOC
09/28/98
| 1 Original
page 1 of 2
XI Amended
Client:
Pacific Environmental Services, Inc.
560 Hemdon Parkway, Suite 200
Hemdon Virginia 20170-5240
Project No.: WO#384
Description: Mass Loss Study for Pacific
Environmental
Report Distribution: Mr. Frank Phoenix
Sample No.: See Below
Date Received: 8/18/98
Sample Description: "See Below
Technical Responsibility ^
Name Tim Clark * >
Title: Laboratory Technician
Signature: _j££-^?~"~^
Date: ?/3-«/
-------
TEST REPORT
Test Report No.:
Report Date:
ADVANCED^^SPHALT TECHNOLOGIES
LABORATORY AND TECHNICAL SERVICES
03840004.DOC
09/28/98
| | Original
X I Amended
page 2 of 2
RAP Samples Test Results
PES Sample
ID#
RAB2B
RAB2E
RAB3B
RAB3M1
RAB3M2
RAB3M3
RAB3E
RAB4B
RAB5B
RAB6B
RAB6E
AA T Sample
ID*
FS481.1
FS482. 1
FS483. 1
FS484. 1
FS485. 1
FS486. 1
FS487. 1
FS488. 1
FS489. 1
FS490. 1
FS491.1
Asphalt
Content, %
ASTM D2172
4.67
5.13
5.27
Moisture
Content, %
1.90
2.25
2.61
1.90
2.52
3.25
2.04
2.56
2.75
3.22
2.73
Advanced Asphalt
Technologies, IP
108 POWERS COURT, SUITE 100
STERLING, VA 20166-9321
PH (800)3956686
PH (703)4444200
FX (703) 444 4368
-------
APPENDIX B.9
VELOCITY OF AIR ACROSS TOP OF
TRANSPORT TRUCKS DURING LOAD-OUT
\O&
-------
VELOCITY OF AIR ACROSS TOP OF TRANSPORT TRUCKS DURING LOAD-OUT
Air velocity measurements were taken above seven transport trucks inside the tunnel
during load-out from Silo No. 2. Measurements were taken using a hot wire anemometer at
five regularly spaced spaced intervals just above the back end of the truck bed. In each case,
a second truck was waiting at the entrance of the tunnel. The results are summarized in
Table T.I below. Refer to Figure 1 for the exact locations of the measuring points and
numbering scheme.
TABLE T.I
AIR VELOCITY OVER TRUCKS SUMMARY
Test
Date
7/24/98
7/24/98
7/25/98
7/25/98
Point
No.
1
2
3
4
5
1
2
3
4
5
1
2
3
4
5
1
2
3
4
L_ 5
Time
of
Reading
1209
1209
1209
1213
1213
1219
1219
1216
1216
1216
1209
1209
1211
1211
1211
1220
1220
1215
1215
1215
Truck
No.
29
29
29
16
16
TP
TP
88
88
88
21
21
7
7
7
15
15
8
8
8
Velocity
Reading
fpm
60
52
59
271
220
71
21
140
135
170
104
135
136
123
72
43
41
64
55
71
-------
Readings taken just above rear of truck bed
168"
116"
64"
CD O
Side View
Five reading points 12 inches above rear door
54321
12"'
I ! ! I
96"
II II
Back View
Figure 1 Velocity Measurement Locations and Dimensions for Transport Trucks
103
-------
APPENDIX B. 10
METALS ANALYSIS OF PROCESS SAMPLES
-------
CASE NARRATIVE
Analysis of Samples for the Presence of Trace Metals
Methods
6010A
7470
Rev.l (7/92)
Rev.O (9/86)
Client:
TLI Project Number:
Date:
Pacific Environmental Services
46705A
September 23, 1998
This report should only be reproduced in full.
Any reproduction of this report requires permission from
Triangle Laboratories, Inc.
Rev. 25-Sep-96
Triangle Laboratories, Inc.
801 Capltola Drive P.O. Box 13485
Durham, NC 27713-4411 Research Triangle Park, NC 27709-3485
919-544-5729 Fax #919-544-5491
-------
Triangle Laboratories, Inc. September 23,1998
Case Narrative TLI Project #: 46705A
Overview
Seven samples were analyzed for arsenic (As), beryllium (Be), cadmium (Cd), cobalt
(Co), chromium (Cr), manganese (Mn), nickel (Ni), lead (Pb), antimony (Sb),
selenium (Se), and mercury (Hg). For all analyses (except Hg), the samples and
associated QC samples were prepared by hotplate digestion following the guidelines of
EPA SW-846 Method 3050A. The samples and associated QC samples for the analysis
of Hg were prepared following the guidelines of EPA SW-846 Method 7471 Rev.O
(9/86). The samples were analyzed following the guidelines of EPA SW-846 Methods
6010A Rev. 1 (7/92), 7471 Rev. 0 (9/86). Results reported relate only to the items
tested.
OC Remarks
The release of this set of data by Triangle Laboratories, Inc. was authorized by the
Quality Control Chemist who has reviewed each sample data package individually
following a series of inspections/reviews. When applicable, general deviations from
acceptable QC requirements are identified below and comments are made on the effects
of these deviations upon the validity and reliability of the results. Specific QC issues
associated with this particular project are:
Sample Receipt:
Three aggregate samples, four liquid AC and three asphalt cement samples were received
at 25 °C on September 15, 1998 in good condition. These samples were received in a box
instead of a cooler. Only seven samples were analyzed for this particular project.
Sample Preparation:
Laboratory documentation of the sample preparation is included in the data package.
Instrumentation:
Arsenic (As), beryllium (Be), cadmium (Cd), cobalt (Co), chromium (Cr), manganese
(Mn), nickel (Ni), lead (Pb), antimony (Sb), selenium (Se), concentrations were
determined by Inductively Coupled Plasma Emission Spectroscopy (ICP).
The linear range for the instrument TJA 61E Trace Analyzer was based on four
standards and a blank, which established a correlation coefficient value greater than or
equal to 0.995. A calibration curve, based on a blank and one standard, is established
for each analytical run, followed by a check high standard and an initial calibration
verification (ICV). The check high standard does not deviate from the calibration
curve by more than 5 %. In addition, continuing calibration verifications (CCVs) are
performed throughout the analytical run.
101
-------
Triangle Laboratories, Inc. September 23,1998
Case Narrative TLI Project #: 46705A
A Reporting Detection Limit (RDL) is used instead of an Instrument Detection Limit
(IDL). The spectrometer and atomic absorption instruments can achieve low detection
limits between 0.2-8 ppb levels for many analytes. Triangle Labs is using RDL values
of 1-10 times the IDL as detection limits for reporting purposes.
Data Review:
All analytes found in the method blank (MB) are detected at a level equal to or less
than the respective Reporting Detection Limit (RDL) except Ni and Pb. The following
guidelines may be used to assess analyte concentrations relative to the method blank: 1.
Analyte quantitations should be considered valid if the level of blank contamination is
less than five percent of the level detected in the field sample, 2. Analyte quantitations
should be considered estimated if the analyte level in the sample is five to twenty times
the level of the analyte in the blank, or 3. Analytes whose level hi a sample is the same
as or less than five times the level detected in the associated blank should be considered
present likely due to laboratory contamination and not native to the sample.
The sample results are based on dry weight.
A sampling date was not supplied by the client and the sampling to analysis holding
times cannot be determined. All samples were analyzed within 7 days of sample
receipt at Triangle Laboratories.
The pre-digestion spike duplicate (MSD) for Mn, Ni, and Pb for the sample
RAP2B/AC demonstrated percent recoveries outside the QC criteria which may
indicate significant matrix effects specific to these analytes hi the native sample matrix.
Please note that the pre-digestion spike (MS) and the post-digestion spike (PDS) met
QC criteria for Mn, Ni, and Pb for sample RAP2B/AC.
The duplicate analyses for Ni for the sample AC IB demonstrated a RPD outside the
QC criteria of 20.0 percent, which indicates the presence of a significant amount of
interferents specific to this analyte in the native sample matrix.
QC requirements:
The analytical duplicates for analytes analyzed by ICP cannot be considered valid
qualifiers if the concentrations of the analytes in the original and/or duplicate sample
are not at least ten times the respective RDLs. The RPDs for these analyses are
indicated by "
-------
Triangle Laboratories, Inc. September 23,1998
Case Narrative TLI Project #: 46705A
The serial dilution analyses for analytes analyzed by ICP cannot be considered valid
qualifiers if the concentrations of the analytes in the serial dilution sample are less than
ten times the respective RDLs. The serial dilution RPDs for these analyses are
indicated by "
-------
STANDARD CONCENTRATIONS
for the TJA 61E TRACE ANALYZER
Analyte
Cd
Co
Cu
K
Mg
Mo
Ni
Pb
•S6I
Se
Sr
Tl
Zn
Units
Ppb
ppb
Ppb
ppb
ppb
JffiL
JffiL
ppb
High Std
1000
1000
'1000
10000
1000
1000
1000
1000
•• A '"i.^
* Vw
1000
1000
1000
1000
1000
ICV/CCV
500
500
500
5000
500
500
500
500
500
500
500
500
ICSAB RDL
500 - 1
500
500
I50Q-
500
19000
500000
500
500
500
500
650
500
500
220
30
12
Wavelength
3130
2265
2286
3247
7664
2790
2020
2316
2203
1960
4215
1908
2062
Note: Use this reference page to review the raw data from the TJA 61E Trace Analyzer.
This page includes the standard concentrations for the check high standard, initial calibration
verification (ICV), continuing calibration verification (CCV), and the interference check solution
(ICS AB). In addition the reporting detection limit (RDL) and wavelength^re reported for each
analyte.
Revision Date: 05-May-98
110
-------
^S^^%;r?r --,.
- *• ABBREVIATIONS
BH = Back Half
COB = Continuing Calibration Blank
CCV = Continuing Calibration Verification
CHECK HS = Check High Standard
D = DUP = Analytical Duplicate (Prepared Duplicate)
DA = Duplicate Analysis
Hi = Front Half
FV = Final Digestate Volume
ICB = Initial Calibration Blank
ICV = Tm'rinl Calibration Verification
ICSAB = Interference Check Solution (Solution AB)
v\ I = Initial
. V £= Final •
Solution AB contains common interferents in addition to the analyte of interest.
DDL = Instrument Detection Limit
L = Serial Dilution
LCS = Laboratory Control Spike Sample
MB = Method Blank
MPV = Mercury Preparation Volume
MS = Pre-digestio n S pike
MSD = Pre-digestio n Spike Duplicate
N/A = Not Applicable
N/Av = Not Available
N/V = Not Valid
PDS = Post-digestion Spike
%REC = Percent Recovery
RDL = Reporting Detection Limit
RPD = Relative Percent Difference
T = Analytical Triplicate (Prepared Triplicate; for Hg analysis by Method 7471 only)
TV = Total Sample Volume
< = Analyte concentration in the sample is less than the respective RDL
\\\
-------
CALCULATIONS FOR SOLID SAMPLES
RESULTS FOR TRACE METALS (except mercury);
RESULT in mg/Kg = \is/L * ml FV * DF
gram WT used* 1000
mi FV = final volume in ml
DF = Dilution Factor
RESULTS FOR MERCURY (He):
RESULT in mg/Kg= ug/L * MPV * DF
gram WT used
MPV = Mercury Preparation Volume = 0.1 L or 0.008 L
DF=sDforJon Factor
%REC (Percent Recovery) for MS/MSD and Hg spikes;
t %REC = Spike sarnpfe Tpsnfrg - original ^TTFP^ results * 100
true spike sample results
%REC (Percent Recovery) forPDS;
%REC = -5t"Tre «nppfe COOC. [Ig/L - ongr^al sample cone. \igfL * 100
spike cone. fig/L
%REC (Percent RecoTerv) forLCS/LCSD:
%REC = Spike sampte cone. tig/L * 100
spike cone. ug/L
RPD= 1 Result 2-Result 1 I * 100
(Result 2 -I-Result l)/2
Rev. 10/10/95 ,
\l-z-
-------
TRIANGLE LABORATORIES, INC
LIST OF CERTIFICATIONS AND ACCREDITATIONS
ENVIRONMENTAL
American Association for Laboratory Accreditation. Accredidation pending. Certificate
Number 0226-01. Accreditation for technical competence in Environmental Testing. (Including
Waste Water, Sol/Haz Waste, Pulp/Paper, and Air Matrices) Parameters are AOX/TOX, and
Dioxin/Furan. Method 1613 for Drinking Water Currently re-applying..
State of Alabama, Department of Environmental Management. Expires December 31, 1998.
Laboratory I.D. # 40950. Dioxin in drinking water.
State of Alaska, Department of Environmental Conservation. Expires December 21, 1998.
Certificate number OS-006-98. Dioxin in drinking water.
State of Arizona, Department of Health Services. Expires May 26, 1998. Certificate
#AZ0423. Drinking Water for Dioxin, Dioxin in WW and S/H Waste. Currently appying for
renewal.
•
State of Arkansas, Department of Pollution Control and Ecology. Expires February 19,
1999. Pulp/paper, soil, water, and Hazardous Waste for Dioxin/Furan; AOX/TOX, Volatiles,
Semi-volatiles, and Metals.
State of California, Department of Health Services. Expires August 31, 1999. Certificate
#1922. Selected Metals in Waste Water, Volatiles, Semi-volatiles, and Dioxin/furan in WW and
Sol/Haz Waste. Dioxin in drinking water.
State of Connecticut, Department of Health Services. Expires September 30, 1999.
Registration #PH-0117. Dioxin in drinking water.
Delaware Health and Social Services. Expires December 31, 1998. Certificate #NC 140.
Dioxin in drinking water.
Florida Department of Health and Rehabilitative Services. Expires June 30, 1998. Dioxin in
SDW. Drinking Water ID HRS# 87424. Pending new certificate.
Triangle Laboratories, Inc.
' 801 Capitola Drive P.O. Box 13485
w™»rfifiMrtiio*«««, Durham, NC 27713-4411 Research Triangle Park,-NO27709-348i
^certific\certlistmem ^ 919-544-5729 Fax#9i9-s44-S49i _.
-------
Hawaii Department of Health. Expires March 1, 1999. Dioxin in drinking water. "Accepted"
status for regulatory purposes.
Idaho Department of Health and Welfare. Expires December 31,1998. Dioxin in drinking
water.
State of Kansas, Department of Health and Environment. Expires January 31, 1999.
Method 1613 for drinking water. ID #'s - Drinking water and/or pollution control - E-10215.
Solid or Hazardous Waste - E-l01209.
Commonwealth of Kentucky, Department for Environmental Protection.
Expires December 31, 1998. JD#90060. Dioxin in drinking water.
Maryland Department of Health and Mental Hygiene. Expires September 30, 1998.
Certification #235 Drinking water by Method 1613 A. Currently applying for renewal.
State of Michigan, Department of Public Health. Expires June 30, 1999. Drinking water by
Method 1613. Current certification is extended, based on New York certificate renewal.
Mississippi State Department of Health. No expiration date. Dioxin in drinking water. ~~
Montana Department of Health and Environmental Services. Expires December 31, 1998.
Dioxin in drinking water. '
State of New Jersey, Department of Environmental Protection and Energy. Expires June 30,
1998. Extended until July 31, 1998 per letter dated May 29, 1998. ID #67851. BNAs and
Volatiles. Dioxin in drinking water. Currently applying for renewal.
State of New Mexico, Environment Department Still certified, awaiting information from
A2LA Dioxin in drinking water.
New York State Department of Health. Received updated certificates. ID #11026.
Environmental Analyses of potable water, non-potable Water, Solid and Hazardous Waste.
Method 1613 in DW.
State of North Carolina, Department of Environment Health and Natural Resources
Expires. August 31,1998. Certificate # 37751. Dioxin in drinking water.
State of North Carolina, Department of Environment, Health, and Natural Resources,
Division of Environmental Management Expires December 31, 2000. Certificate # 485.
Metals, pesticides & PCBs, semi-volatiles and volatiles; TCLP.
RcviMd 8/3/98 On
y:certific\certlist.mem
IK
-------
North Dakota State Department of Health and Consolidated Laboratories. Expires
December 31, 1998. Certificate # R-076. Effective October 4,1993. Dioxin in drinking water.
Oklahoma Department of Environmental Quality. Expires August 31, 1998. Laboratory
#9612. Dioxin by 1613 A, 8290 and 8280. Submitted renewal application 7/1.
State of South Carolina, Department of Health and Environmental Control. Expires
June 30, 1998. Extended August 31, 1999. Certificate number #99040001 (drinking water).
Expires August 31,1999. Certificate number #99040002 (other parameters). Dioxin/Furans,
BNA, Volatiles, and PCBs/pesticides under Clean Water Act, 2,3,7,8-TCDD for Drinking Water,
and Organic extractables for Solid and Hazardous Waste.
State of Tennessee. Department of Environment and Conservation. Expires
February 5, 1999. ED #02992. Method 1613 Drinking water only.
U.S. Department of Agriculture Soil Permit Expires September 30, 2001. Permit No. S-
3790. Under the authority of the Federal Plant Pest Act, permission is granted to receive foreign
soil samples for use in laboratory analysis.
U.S. Army Corps of Engineers. Expires October 19, 1999. Validated to perform analyses for
the Fort Belvoir, VA (Contract Number DACA31-97-D-0029), Vint Hill Farms Station, Vint Hill,
VA (Contract Number DACA31-95-D-0083), and Selma Pressure Treating Superfund Site,
Selma, CA (Contract number DACW45-94-D-0054).
U.S. EPA Region V. Expires November 14, 1999. Dioxin in drinking water.
U.S. EPA Region VTTI, for the State of Wyoming. Expires November 12, 1998. Dioxin in
drinking water.
State of Utah, Department of Health. Expires May 30,2000. Certificate Number E-166.
Certification for the following parameters: Semi-Volatiles and Volatiles under RCRA; Volatiles
under Clean Water Act; Dioxin/furans by Method 8280; Drinking water for Dioxin by Method
1613; Metals including Mercury and Microwave Digestion.
Commonwealth of Virginia, Department of General Services, Division of Consolidated
Laboratory Services. Expires June 30, 1999. ID # 00341. Dioxin in drinking water.
State of Washington, Department of Ecology. Expires September 11, 1998. Lab
Accreditation Number C067. Scope of Accreditation applies to water analyses for
R*viMd 8/3/98 d»
y:certific\certlist.mem
10
-------
Polychlorinated Dibenzo-p-dioxins and Polychlorinated Dibenzofurans, BNA Extr (Semivolatile)
Organics and Purgeable (Volatile) Organics.
State of Washington, Department of Health. Expires April 30, 1999. Dioxin in drinking
water. Lab I.D. 129.
State of West Virginia, Department of Health. Expires December 31, 1998. Certificate No.
9923(C). Dioxin in drinking water.
State of Wisconsin, Department of Natural Resources. Expires August 31,1998. Laboratory
ID Number 999869530. Certification for the following categories of Organics: Purgeable,
Base/Neutral, Acid, PCBs, and Dioxin. Expires November 14, 1999. Laboratory ID 999869530.
Dioxin in drinking water.
PHARMACEUTICAL
Drug Enforcement Agency (DEA). Expires November 30, 1998. Registration number
RT01195835. Controlled substance registration for schedules 1,2,3,3N,4,5.
N.C. Department of Human Resources. Expires October 31, 1998. Registration number
NC-PT 0000 0031. North Carolina controlled substances registration. Application submitted for
renewal.
Food & Drug Administration (FDA) Registration. Expires June 1998. ID #'s 001500
1053481. Annual registration of drug establishment.
OTHER
Clinical Laboratory Improvement Amendments (CLIA) Registration. Expires May 30,
1999. ID#34D0705123. Department of Health & Human Services, Health Care Financing
Administration.
U.S. EPA Large Quantity Hazardous Waste Generator. No expiration date. EPA ED
#NCD982156879. Permit indicates that the laboratory is a large generator of hazardous waste.
North Carolina General License for Radiation Protection. No expiration date. No License.
032-875-OG. The general license applies only to radioactive material contained in devices which
have been manufactured and labeled in accordance with specific requirements.
RoviMd 8/3/98 _ ~
11
-------
DOCUMENT
CONTROL
in
901 Capitate
Ourtara, HC 27713*t*rt
919-344-S729
-------
Client: Pacific Environmental Services
Project Number: 46705A
Sample Report
Client Sample ID:
TLI Sample ID:
Date Received:
Date Prepared:
Date Analyzed:
Matrix:
AC1B
218-12-1
September 15. 1998
September 21, 1998
September 22. 1998
SOLID
"° -. - , . " ;'?:&s*" -
" ' ' '•'*-"* $'
Analvte '•'•'
As
Be
Cd
Co
Cr
Mn
Ni
Pb
Sb
Se
<*• Coneys?
(uo/L) :
-0.823
-0.021
-0.192
4.867
0.204
1.375
210.290
6.186
1.250
5.179
jffSrarns:^ .
Submitted
N/A
N/A
N/A
N/A
N/A
N/A
N/A
N/A
N/A
N/A
•-* "--grams *r
;-Used ;
0.609
0.609
0.609
0.609
0.609
0.609
0.609
0.609
0.609
0.609
v-^mL>£"
Final Vol.
100
100
100
100
100
100
100
100
100
100
: Dilution v
Factor *
1
1
1
1
1
1
1
1
1
1
- mg/Kg
Result
< 0.821
< 0.164
< 0.164
0.799
< 0.328
< 0.328
34.5
1.02
< 0.657
0.850
1
Triangle Laboratories, Inc.
801 Capitola Drive * Durham, North Carolina 27713
Tele: (919) 544-5729 * Fax: (919) 544-5491
Printed: 23-Sep-98 at 03:59 PM
-------
Client: Pacific Environmental Services
Project Number; 46705A
Sample Report
Client Sample ID:
TLI Sample ID-
Date Received:
Date Prepared:
Date Analyzed:
Matrix:
AC1B
218-12-1 D
September 15. 1998
September 21, 1998
September 22. 1998
SOLID
'"**% ' - v"> ' -"'&••' "'^Wfcfc"
>'•:--- , -«'--"f5**.;
Anatyte.
As
Be
Cd
Co
Cr
Mn
Ni
Pb
Sb
Se
-'.;•. T-GOnCfeSs*
':-(uti/L>«.:
-2.709
-0.118
-0.206
0.633
-0.359
0.731
49.276
2.919
0.148
0.983
*SuBmitt^
N/A
N/A
N/A
N/A
N/A
N/A
N/A
N/A
N/A
N/A
^^graiTO/^
feilffUsecf-^
0.647
0.647
0.647
0.647
0.647
0.647
0.647
0.647
0.647
0.647
Ui-fnL^
RnaTVofcr
100
100
100
100
100
100
100
100
100
100
•^nufor^JI
--•I" Factor M*
1
1
1
1
1
1
1
1
1
1
4>mg/Ka-;aV
- Result
< 0.773
< 0.155
< 0.155
< 0.309
< 0.309
< 0.309
7.62
0.451
< 0.618
< 0.464
Triangle Laboratories, Inc.
801 Capitola Drive * Durham, North Carolina 27713
Tele: (919) 544-5729 * Fax: (919) 544-5491
Printed: 23-Sep-98 at 03:59 PM
\\<\
14
-------
Client: Pacific Environmental Services
Project Number: 46705A
Sample Report
Client Sample ID:
TLI Sample ID:
Date Received:
Date Prepared:
Date Analyzed:
Matrix:
AC2B
218-12-2
September 15. 1998
September 21, 1998
September 22. 1998
SOLID
K~-V. .•*y"f&?y.r
•A :."%£
Analvte >*
As
Be
Cd
Co
Cr
Mn
Ni
Pb
Sb
Se
t^ilGonc.*!-
^;.(ua/Lrr
-1.444
-0.110
-0.220
8.019
1.034
4.448
291.857
3.106
-2.120
5.196
•^rams;;3»
Submitted
N/A
N/A
N/A
N/A
N/A
N/A
N/A
N/A
N/A
N/A
fijk grams^
:;>- Used ;^
0.514
0.514
0.514
0.514
0.514
0.514
0.514
0.514
0.514
0.514
sismL ^ ,;
RnalVoI.
100
100
100
100
100
100
100
100
100
100
Diiufon,.,,
Factor
1
1
1
1
1
1
1
1
1
1
4img/Kg i
Result *
< 0.973
< 0.195
< 0.195
1.56
< 0.389
0.865
56.8
0.604
< 0.778
1.01
Triangle Laboratories, Inc.
801 Capitola Drive * Durham, North Carolina 27713
Tele: (919) 544-5729 * Fax: (919) 544-5491
Printed: 23-Sep-98 at ~ 03:59 PM
|2
-------
Client: Pacific Environmental Services
Project Number: 46705A
Sample Report
Client Sample ID:
TLI Sample ID:
Date Received:
Date Prepared:
Date Analyzed:
Matrix:
RAP2B/AC
218-12-3
September 15. 1998
September 21, 1998
September 22. 1998
SOLID
Analvte - ,
As
Be
Cd
Co
Cr
Mn
Ni
Pb
Sb
Se
^~ •-*- :"' -/ttnfjS' ' Vs'si*'» •-
(U
-------
Client: Pacific Environmental Services
Project Number: 46705A
Sample Report
Client Sample ID:
TLI Sample ID:
Date Received:
Date Prepared:
Date Analyzed:
Matrix:
RAP2B/AC
218-12-3 L
September 15. 1998
September 21. 1998
September 22. 1998
SOLID
Analvte '
As
Be
Cd
Co
Cr
Mn
Ni
Pb
Sb
Se
•f&ftaPfZisi
%ia/LK^
0.864
-0.149
0.054
1.198
0.387
10.772
47.382
6.109
0.165
1.116
u--s||grarns ^
Submitted ?
N/A
N/A
N/A
N/A
N/A
N/A
N/A
N/A
N/A
N/A
r^flrarosdg:
••>l--Userff>-
0.576
0.576
0.576
0.576
0.576
0.576
0.576
0.576
0.576
0.576
^Rraivai-
100
100
100
100
100
100
100
100
100
100
;>JD|0Bonpf
*• -Factor '-•'"
5
5
5
5
5
5
5
5
5
5
. ^ssyHBflte 'UK
' -Result -3?.
< 4.34
< 0.868
< 0.868
< 1.74
< 1.74
9.35
41.1
5.30
< 3.47
< 2.60
*" - ' i
Triangle Laboratories, Inc.
801 Capitola Drive * Durham, North Carolina 27713
Tele: (919) 544-5729 * Fax: (919) 544-5491
Printed: 23-Sep-98 at 03:59 PM
17
-------
Client: Pacific Environmental Services
Project Number; 46705A
Sample Report
Client Sample ID:
TLI Sample ID:
Date Received:
Date Prepared:
Date Analyzed:
Matrix:
RAP2B/AC MS
218-12-3 MS
September 15. 1998
September 21. 1998
September 22. 1998
SOLID
Analvte -:
As
Be
Cd
Co
Cr
Mn
Ni
Pb
Sb
Se
?;'*tucia-} r*#
45.259
45.643
45.860
49.917
48.552
95.805
262.042
75.086
46.222
47.150
N/A
N/A
N/A
N/A
N/A
N/A
N/A
N/A
N/A
N/A
0.534
0.534
0.534
0.534
0.534
0.534
0.534
0.534
0.534
0.534
100
100
100
100
100
100
100
100
100
100
1
1
1
1
1
1
1
1
1
1
8.48
8.55
8.59
9.35
9.09
17.9
49.1
14.1
8.66
8.83
Triangle Laboratories, Inc.
801 Capitola Drive * Durham, North Carolina 27713
Tele: (919) 544-5729 * Fax: (919) 544-5491
Printed: 23-Sep-98
18
-------
Client: Pacific Environmental Services
Project Number; 46705A
Sample Report
Client Sample ID:
TLI Sample ID:
Date Received'
Date Prepared:
Date Analyzed:
Matrix:
RAP2B/AC MSD
218-12-3MSD
September 15. 1998
September 21, 1998
September 22. 1998
SOLID
Anatyte
As
Be
Cd
Co
Cr
Mn
Ni
Pb
Sb
Se
v?»&
(uo/LV^"
43.250
46.674
46.595
47.721
48.170
59.290
84.610
55.565
47.180
43.921
^QI'J^TO tajSC-
N/A
N/A
N/A
N/A
N/A
N/A
N/A
N/A
N/A
N/A
0.552
0.552
0.552
0.552
0.552
0.552
0.552
0.552
0.552
0.552
100
100
100
100
100
100
100
100
100
100
.
•"4'X,FactOFi*«
1
1
1
1
1
1
1
1
1
1
-
» %'feRestit ' ff'~*--
7.84
8.46
8.44
8.65
8.73
10.7
15.3
10.1
8.55
7.96
Triangle Laboratories, Inc.
801 Capitola Drive * Durham, North Carolina 27713
Tele: (919) 544-5729 * Fax: (919) 544-5491
Printed: 23-Sep-98 at 04:55 PM
19
-------
Client: Pacific Environmental Services
Project Number; 46705A
Sample Report
Client Sample ID:
TLI Samole ID:
Date Received:
Date Prepared:
Date Analyzed:
Matrix:
AC3B
218-12-5
September 15. 1998
September 21, 1998
September 22. 1998
SOLID
Analvte
As
Be
Cd
Co
Cr
Mn
Ni
Pb
Sb
Se
; v-€oncL'-v;
'•ftnJLV'--
-3.235
-0.118
-0.288
0.196
-0.602
1.017
26.323
2.282
1.523
0.861
ssgrams .
Submitted
N/A
N/A
N/A
N/A
N/A
N/A
N/A
N/A
N/A
N/A
,;v,.grams,,^.
-•"•-"Used •?-
0.504
0.504
0.504
0.504
0.504
0.504
0.504
0.504
0.504
0.504
; ,:;tnL
Final Vol.
100
100
100
100
100
100
100
100
100
100
^Dilution;
Factor
1
1
1
1
1
1
1
1
1
1
: y mg/Kg
Result •
< 0.992
< 0.198
< 0.198
< 0.397
< 0.397
< 0.397
5.22
0.453
< 0.794
< 0.595
-
Triangle Laboratories, Inc.
801 Capitola Drive * Durham, North Carolina 27713
Tele: (919) 544-5729 * Fax: (919) 544-5491
Printed: 23-Sep-98 at 03:59 PM
PO
-------
Client: Pacific Environmental Services
Project Number: 46705A
Sample Report
Client Sample ID:
TLI Sample ID:
Date Received:
Date Prepared:
Date Analyzed:
Matrix:
RAP3M2/AC
218-12-6
September 15. 1998
September 21, 1998
September 22. 1998
SOLID
Analvfie ; '•
As
Be
Cd
Co
Cr
Mn
Ni
Pb
Sb
Se
:-r-?Cdac£K»
Kioto T;;
-2.215
-0.194
0.040
0.072
-0.083
13.105
39.449
14.295
0.085
-0.075
1 Ifcf 'aHSnjSr^iii
'Submffltef'
N/A
N/A
N/A
N/A
N/A
N/A
N/A
N/A
N/A
N/A
iǤ4Jjrarris'|i|
0.644
0.644
0.644
0.644
0.644
0.644
0.644
0.644
0.644
0.644
^RnalMI
100
100
100
100
100
100
100
100
100
100
r vKOBuBpn;^
; -"''Factor"'
1
1
1
1
1
1
1
1
1
1
•"
-Jtmg/Kg Kit:
%Resuft'^-
< 0.776
< 0.155
< 0.155
< 0.311
< 0.311
2.03
6.13
2.22
< 0.621
< 0.466
Triangle Laboratories, Inc.
801 Capitola Drive * Durham, North Carolina 27713
Tele: (919) 544-5729 * Fax: (919) 544-5491
Printed: 23-Sep-98 at 03:59 PM
-------
Client: Pacific Environmental Services
Project Number; 467Q5A
Sample Report
Client Sample ID:
TLI Sample ID:
Date Received:
Date Prepared:
Date Analyzed:
Matrix:
AC4B
218-12-8
September 15. 1998
September 21, 1998
September 22. 1998
SOLID
•• * - Ans^rtei-?*?
As
Be
Cd
Co
Cr
Mn
Ni
Pb
Sb
Se
;4:^Cona^i|
" t* -: • " -"'"«"V .-**
:•/ Oig/U **
-2.262
-0.209
-0.259
0.208
-0.195
1.354
46.037
1.640
0.630
0.907
.-^.srarns ^
Submitted
N/A
N/A
N/A
N/A
N/A
N/A
N/A
N/A
N/A
N/A
sv- grams ;v
:^tJsedf.Y;
0.528
0.528
0.528
0.528
0.528
0.528
0.528
0.528
0.528
0.528
; >:,.,; : mL - ji;;
- RnalVoi;
100
100
100
100
100
100
100
100
100
100
-Dilution, '
Factor
1
1
1
1
1
1
1
1
1
1
.'.« mg'Kg
Result ;
< 0.947
< 0.189
< 0.189
< 0.379
< 0.379
< 0.379
8.72
< 0.379
< 0.758
< 0.568
Triangle Laboratories, Inc.
801 Capitola Drive * Durham, North Carolina 27713
Tele: (919) 544-5729 * Fax: (919) 544-5491
Printed: 23-Sep-98 at 03:59 PM
-------
Client: Pacific Environmental Services
Project Number: 46705A
Sample Report
Client Sample ID:
TLI Sample ID:
Date Received:
Date Prepared:
Date Analyzed:
Matrix:
RAP5B/AC
218-12-9
September 15. 1998
September 21, 1998
September 22. 1998
SOLID
Analvte
As
Be
Cd
Co
Cr
Mn
Ni
Pb
Sb
Se
Cone. ..,
fuo/L)
-3.079
-0.209
-0.250
-0.429
-0.315
8.609
13.783
5.878
1.454
0.699
,.#, grams ,,
Submitted
N/A
N/A
N/A
N/A
N/A
N/A
N/A
N/A
N/A
N/A
: r:4Jraras .,
•v~tfeiar?s
0.532
0.532
0.532
0.532
0.532
0.532
0.532
0.532
0.532
0.532
. , .- jjpL^if,
FinafVoll:'
100
100
100
100
100
100
100
100
100
100
rtDHu#on ,
1 "'•*' Factor ''^
1
1
1
1
1
1
1
1
1
1
-
;^mg/Kg
'"-Result
< 0.940
< 0.188
< 0.188
< 0.376
< 0.376
1.62
2.59
1.10
< 0.752
< 0.564
Triangle Laboratories, Inc.
801 Capitola Drive * Durham, North Carolina 27713
Tele: (919) 544-5729 * Fax: (919) 544-5491
Printed: 23-Sep-98 at 03:59PM
23
-------
Client: Pacific Environmental Services
Project Number; 46705A
QA: Serial Dilution
Client Sample ID:
TLI Sample ID:
Date Prepared:
Date Analyzed:
Matrix:
RAP2B/AC
218-12-3
September 21. 1998
September 22. 1998
SOLID
RAP2B/AC
218-12-3 L
September 21. 1998
September 22. 1998
SOLID
AnaMe
As
Be
Cd
Co
Cr
Mn
Ni
Pb
Sb
Se
Native Sample
*<'-"•' - "--rra/Kicr^
< 0.868
< 0.174
< 0.174
0.585
< 0.347
9.20
40.7
5.38
< 0.694
0.650
*&* uq/L-t%";
1.245
-0.167
0.238
3.371
1.630
52.992
234.393
31.007
0.594
3.746
Serial Dilution
:*$|Cbw ^~'*3&*)&^sJm;
Hfc-
< 4.34
< 0.868
< 0.868
< 1.74
< 1.74
9.35
41.1
5.30
< 3.47
< 2.60
^•sJPllj^-sW '*; •- «• •
v*%Gorjrr!>^
0.864
-0.149
0.054
1.198
0.387
10.772
47.382
6.109
0.165
1.116
'^RPEX '
?--:Wtfi:^
-------
Client: Pacific Environmental Services
Project Number: 46705A
QA: Duplicate
Client Sample ID:
TLI Sample ID4
Date Prepared'
Date Analyzed:
Matrix:
AC1B
218-12-1
September 21. 1998
September 22. 1998
SOLID
AC1B
218-12-1 D
September 21. 1998
September 22. 1998
SOLID
- , «- j T
/vZ^-'V^""^ s" '-'
Anaivte
As
Be
Cd
Co
Cr
Mn
Ni
Pb
Sb
Se
—
Sample
i ;>^';, .i jng/K3?.4
I''-" :'~-"" Result
< 0.821
< 0.164
< 0.164
0.799
< 0.328
< 0.328
34.5
1.02
< 0.657
0.850
gfe^wf
fS-^Dbnc^
-0.823
-0.021
-0.192
4.867
0.204
1.375
210.290
6.186
1.250
5.179
Duplicate
< 0.773
< 0.155
< 0.155
< 0.309
< 0.309
< 0.309
7.62
0.451
< 0.618
< 0.464
m^lCotKL?ff^
-2.709
-0.118
-0.206
0.633
-0.359
0.731
49.276
2.919
0.148
0.983
-------
Client: Pacific Environmental Services
Project Number: 46705A
OA: Matrix Spikes (Pre-Digestion)
Client Sample ID:
TLI Sample ID:
Date Prepared:
Date Analyzed:
Matrix:
RAP2B/AC MS
218-12-3 MS
September 21, 1998
September 22, 1998
SOLID
RAP2B/AC MSD
218-12-3 MSD
September 21, 1998
September 22, 1998
SOLID
Analvte
As
Be
Cd
Co
Cr
Mn
Ni
Pb
Sb
Se
Matrix Spike
Result ^
mo/Ka
8.48
8.55
8.59
9.35
9.09
17.9
49.1
14.1
8.66
8.83
lii^^s**,,-,
'' ma/w
9.37
9.37
9.37
9.37
9.36
9.34
9.37
9.39
9.37
9.36
Recovery
91°/<
91 7<
927<
947<
97°/«
937«
907<
93°/c
927.
877<
Matrix Spike Duplicate
;tfer;k|?sUft^^;
"•''•• - mo/Ka •$":"'"
7.84
8.46
8.44
8.65
8.73
10.7
15.3
10.1
8.55
7.96
.^waSpikeyf
-S'malKa
9.06
9.06
9.06
9.06
9.06
9.02
9.04
9.09
9.06
9.06
- -
Recoveiy
877<
937«
937(
897<
967<
177<
-281 7t
527e
947.
81 7<
-
48SS$*
7.84%
1.06%
1.76%
7.78%
4.04%
50.3%
105%,
33.1%
1.28%
10.4%
—
—
—
—
—
—
—
—
—
— —
—.- '
—
—
—
—
—
—
—
—
—
_.
Triangle Laboratories, Inc.
801 Capitola Drive * Durham, NC 27713
Tele: (919) 544-5729 * Fax: (919) 544-5491
Printed: 23-Sep-98
at
04:55 PM
-------
Client: Pacific Environmental Services
Project Number: 46705A
OA: Matrix Spikes (Post-Digestion)
Client Sample ID:
TLI Sample ID:
Date Prepared:
Date Analyzed:
Matrix:
RAP2B/AC PDS
218-12-3 PDS
September 21, 1998
September 22. 1998
SOLID
Analvte
As
Be
Cd
Co
Cr
Mn
Ni
Pb
Sb
Se
Post-Diq
Recoveretf if
Amount (uqiij
48.71
47.49
47.88
52.03
50.65
102.04
284.51
78.84
48.74
48.69
estion Spike
> :--.^*i,.SpBCff-*>. '*
1 Amount (ug/L)
50
50
50
50
50
50
50
50
50
50
> •*=?%,'£?:
Recovery
97°/<
95°/<
96°/c
97°/<
101%
98°/<
100°/c
96°/«
97°/<
907,
Post-Digestion Spike Duplicate
~: Recovered wit -?•-.
* Amount (uo/L) :
' *?r Spike- -f^
Amount (uo/L)
— _...
% '-
Recovery
_ —
RPD
—
—
—
—
...
...
...
...
...
...
_
...
—
_.
—
—
—
—
—
_
—
—
—
— ..
.. _
—
—
—
—
—
—
Triangle Laboratories, Inc.
801 Capitola Drive * Durham, NC 27713
Tele: (919) 544-5729 * Fax: (919) 544-5491
Printed: 23-Sep-98
at
04:00 PM
27
-------
Client: Pacific Environmental Services
Project Number; 46705A
QA: Method Blank
TLI Sample ID:
Date Prepared:
Date Analyzed:
Matrix:
46705A MB
September 21, 1998
September 22. 1998
N/A
AnaMe
As
Be
Cd
Co
Cr
Mn
Ni
Pb
Sb
Se
Method Blank
Recovered •$
~> •'•>- £&''*. ' ^ *''•<*
Amount (uo/LV
-2.84
-0.18
-0.32
-0.46
-0.33
0.55
-3.91
2.94
1.33
0.22
[ , :!sgeto*6n.;>4 , \ ->•'.'•;&
'•' ' 'Urrifefijotv :'":" • "'*••"'
5
1
1
2
2
2
3
2
4
3
—
—
—
—
—
—
—
—
—.
—
—
—
—
—
—
—
—
—
—
—
—
, :,:,.J- ''-Pass-or
' :-'-:^"rFa?l
Pass
Pass
Pass
Pass
Pass
Pass
Fail
Fail
Pass
Pass
*..
-*_
—
_
— .
...
—
...
...
...
—
—
...
— _
_
~
_
_.
_
—
Triangle Laboratories, Inc.
801 Capitola Drive * Durham, NC 27713
Tele: (919) 544-5729 * Fax: (919) 544-5491
Printed: 23-Sep-98
at
04:00 P!>
28
-------
Client: Pacific Environmental Services
Project Number: 46705A
QA: Lab Control Spikes
TLI Sample ID-
Date Prepared:
Date Analyzed:
Matrix:
46705A LCS
September 21. 1998
September 22, 1998
N/A
Analyte
As
Be
Cd
Co
Cr
Mn
Ni
Pb
Sb
Se
Lab Control Spike
• • • jRepoveragg
Amount (uq/t-f
42.38
51.00
47.41
48.21
48.52
48.62
45.02
49.59
49.26
43.95
" Amount (ucj/D
50
50
50
50
50
50
50
50
50
50
Recovery
85°/<
102%
95°/c
96°/c
977.
97°/<
907<
997.
997.
887<
Lab Control S
• ^Recovered ;<*»• --
**•••* - ''''---.•. ,,
Dike Duplicate
Amdunt^jq/Ly
. -.
i ;.,' a/ •• -
=r^^-y-7wv i*- \
RecovenE
: RPD
—
...
—
„
._
...
__
_
_ .
_.
_ .
_..
_ .
—
_
—
—
—
_
—
_ _:. -
—
—
—
—
—
—
—
—
—
Triangle Laboratories, Inc.
801 Capitola Drive * Durham, NC 27713
Tele: (919) 544-5729 * Fax: (919) 544-5491
Printed: 23-Sep-98
at 04:00 PM
29
-------
Client:
Project Number:
Pacific Environmental Services
46705A
Sample Report
Date Received:
Date Prepared:
Date Analyzed:
DATA FILE:
Matrix:
September 15. 1998
September 22, 1998
September 22. 1998
AB936
SOLID
ANALYTE:
Ha—
uq/LRDL
0.2-
Analvsis Method:
7471
Instrument P E Zeeman 5100
Soike Cone. (uoflJ
5
CVAA ANALYTE SUMMARY REPORT
Client Sample ID
AC1B
AC1BD
AC2B
AC2BD
RAP2B/AC
RAP2B/ACD
AC3B
AC3BD
RAP3M2/AC
RAP3M2/ACD
AC4B
AC4BD
RAP5B/AC
RAP5B/AC D
RAP2B/AC MS
RAP2B/ACMSD
RAP2B/AC MS
RAP2B/ACMSD
Method Blank
Method Blank D
LCS
LCSD
TLI SAMPID
218-12-1
218-12-1 D
218-12-2
218-12-2 D
218-12-3
218-12-3 D
218-12-5
218-12-5 D
218-12-6
218-12-6 D
218-12-8
21 8-1 2-8 D
218-12-9
21 8-1 2-9 D
21 8-1 2-3 MS
218-12-3 MSD
True Spike MS
True Spike MSD
46705AMB
46705AMBD
46705A LCS
46705ALCSD
ug/L
CONG
-0.018
0.010
-0.028
-0.041
-0.034
-0.028
-0.013
-0.005
-0.049
-0.044
-0.018
-0.034
-0.039
-0.052
3.915
4.330
5
5
0.041
-0.003
4.384
4.219
ml
MPV
100
100
100
100
100
100
100
100
100
100
100
100
100
100
100
100
100
100
_
-
_
—
gramwt
USED
0.630
0.630
0.647
0.649
0.680
0.674
0.611
0.613
0.655
0.653
0.654
0.649
0.654
0.649
0.603
0.610
0.603
0.610
_
—
_
—
OIL
FACTOR
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
_
—
_
—
mg/Kg
RESULT
< 0.032
< 0.032
< 0.031
< 0.031
< 0.029
< 0.030
< 0.033
< 0.033
< 0.031
< 0.031
< 0.031
< 0.031
< 0.031
< 0.031
0.649
0.710
0.829
0.820
_
—
__
~™
Avg.
RESULT
< 0.032
_
< 0.031
_
< 0.030
—
< 0.033 "
_.
< 0.031
_
< 0.031
_
< 0.031
-
-
- ~-
-
_
—
RPD
-
__
-
_
-
M
-
„
-
„
-
__
—
8.92%
-
_'
—
_
—
%REC
-
._
-
M
-
•M
-
_
-
^ —
-
_
—
78%
87%
--
„
—
889i
849i
Triangle Laboratories, Inc.
30
-------
.I r rw\'~(rn, z '-u"y .--^
SAMPLE
DATA
*n
Ourimrn, MC 2771^4411
919*444723
P.O. Be* 1348S
FtX* 919-544-5491
tMC 27705
31
-------
-------
OPAC
PACIFIC ENVIRONMENTAL SERVICES, INC.
Central Park West
5001 South Miami Boulevard, P.O. Box 12077
Research Triangle Park, North Carolina 27709-2077
(919) 941-0333 FAX: (919) 941-0234
CM
Sample Chain Of Custody Record
I PLANT: US EPA HOT MIX ASPHALT PLANT C
RECOVERY PERSON: J. Swift
PROJECT NO.: S508.001
SAMPLERS: N/A
Sample
ID
AC1B
AC2B
RAP2B/AC
RAP2B/AGG
AC3B
RAP3M2//
RAP3M2/*
AC4B '
lC
<*<*
RAP5B/KC
RAP5B /A4G
Sample
Name
Liquid AC, Run 1 Begin
Liquid AC, Run 2 Begin
Recycled Asph, Run 2 Begin (Asphalt Cement)
Recycled Asph, Run 2 Begin (Aggregate)
Liquid AC, Run 3 Begin
Recycled Asph Run 3 Middle (Asphalt Cement)
Recycled Asph Run 3 Middle (Aggregate)
Liquid AC, Run 4 Begin
Recycled Asph, Run 5 Begin {Asphalt Cement)
Recycled Asph, Run 5 Begin (Aggregate)
No.
of
Cont.
1
1
1
1,
1
1
1
1
1
1
Relinquished by:
Relinquisned by:
Analytical Request
Metals* using 7000 series (SW-846)
Metals* using 7000 series (SW-846)^
Metals* using 6010/7000 series (SW-846)
Metals* using 6010/7000 series (SW-846)
Metals* using 7000 series (SW-8461
Metals* using 6010/7000 series (SW-846)
Metals* using 6010/7000 series (SW-846)^
Metals* using 7000 series (SW-846)
Metals* using 6010/7000 series (SW-846)
Metals* using 6010/7000 series (SW-846)
Comments
* 11-Sb. As, Be, Cd, Cr, Pb, Mn, Ni. Se, Co,& Hg
* 11-Sb, As, Be, Cd. Cr. Pb. Mn. Ni. Se. Co.& Hq
* 11-Sb^As, Be, CdLCr^Pb, Mn, Nij_Se, Co^ Hg^
* 11-Sb, As. Be, Cd, Cr, Pb, Mn, Ni, Se, Co,& Hg
* 11-Sb, As. Be. Cd, Cr. Pb, Mn, Ni. Se. Co,& Hg
* 11-Sb, As, Be, Cd, Cr. Pb. Mn, Ni. Se, Co.& Hg
* 11-Sb, As. Be, Cd, Cr, Pb, Mn. Ni, Se. Co.& Hg
* 11-Sb, As. Be, Cd, Cr. Pb, Mn. Ni. Se. Co,& Hg
* 11-Sb, As, Be, Cd, Cr, Pb, Mn. Ni. Se, Co,& Hg
* 11-Sb. As. Be. Cd, Cr, Pb, Mn, Ni, Se, Co,& Hg
Date Time Received by:
Date Time Received for Lab by: i
s^^1/ "i- /•/ / o»- — =• /^-/s'^/y y?^,^.
-------
=THIAN(u,E LABORATORIES, INC. -- LOO IN RECORD/CHAIN OF CUSTODY=
| j Custody Seal i Absent Sample Seals i Absent ftn * METALS LAB j
II t ^^TLj'A^S- e*-Jf JVt I
| ' NI— ^/ircr1 9-»6 "1%
II 1
n i
U 1
II 1
II 1 •
» • i
i
n i •
•i • • i
»i
i
« , i
. .i i
To STORAGBj
Date/Init
To LAB
Dal.e/Init
To STORAGE]
Date/Init
,
^
To LAB
Date/Init
"
..
!'
To STORAGE |
Date/Init
To LAB
Date/Init
To STORAGE
Date/Init
-
--
'.
1
DISPOSED
Date/Init
'
t
*.
•
1
1
H Receiving 'Remarks: SAMPLES REC'D IN BOX - NO COOLANT
II . ' bo
, !•: • to
i || 'Archive Remarks: ' —
Form Revised 05/27/1997 -- Page 1 OF 1=
-------
PAGE 1 OF 1
TRIANGLE LABORATORIES, INC. |
Sample Preparation Tracking s Management Form |
ct: 4670SA Client: Pacific Environmental Services (PES03) |
ormation
| TLI /
>| SAMPLE ID / CLIENT
1| / SAMPLE ID
I I
|l^ample |Final |
/Wgt \ Vol | Volume | / /
\ g // ml I ml |
I
| TLI Blank
I
I
TLI Blank |
I®
| 218-12-1
AC1B
i i
i i
218-12-2
AC2B
fell
I I
I I
| 218-12-5
I
AC3B
,5(4'
| 218-12-8
I
AC4B
| 218-12-3
I
RAP2B/AC
toft
| 218-12-6
RAP3M2/AC
\ I
| 218-12-9
I
RAP5B/AC
LCS
I
LAB CONTROL SPIKE |
218-12-1 D
AC1B DUPLICATE
iQWf
I 218-12-3 MS
I AC3B MATRIX SPIKE l
I I
| 218-12-3 MSD
| AC3B MATRIX SPIKE OOP.
I I
REV 07/26/93 (PSTMP 7)--+
34
-------
PAGE
_|05
INORGANICS SPIKE LOG
DATE
PROJECT #
SAMPLE IDs
ANALYTE
ORIGINAL
STANDARD
X
ORIGINAL
STANDARD
CONC.
(PPM)
SPIKE
SAMPLE
(UU
RNAL
VOLUME
(mL)
SPIKE
SAMPLE
(PPB)
INITIALS
WITNESS
1-
LKJ
<3/S-/a-/o MS
V
IDOO
V&
l
ll
-------
___* SEE SPIKE LOG
Project
EXPdate
6/1 /SQ
8/1/96
6/1/99
6/1/99
8/1/99
8/1/99
W1/98
a/i/99
9/1/99
8/1/99
8/1/99
.8/1/99
8/1/99
8/1/99
e/i/99
4/1/99
8/1/99
9/1/99
8/1/99
9/1/99
6/1/99
9/1/99
an/as
a/i /se
8/1/99
8/1/99
8/1/99
8/1/99
8/1/99
8/1/99
Spacing SUndanf P
[torrent Standard Orig. Std.
10 (ppm)
'9
to
U
u
)
3a
to
;a
2a
Id
^5
;r
:u
:a
ra
I
c
Mg
*3
*n
Mo
•la
X«
*
»b
5t>
•*
Ti
n
f
!n
[n
3-64-7
aaw
*«*-7
3«O6
3*4-7
364-7
3404
3«O6
3«0-10
3«oe
3«O«
3-6O8
»«oe
3*O«
*60-9
3*4-7
*4fr5
»«>«
3«>5
3«&e
3«>«
3*4-7
>«X7
»«&«
9408
3-804
woe
3-eofl
3««
3-6O8
3«W
3^0-7
100
100
100
10000
100
100
100
100
10000
100
100
100
100
100
10COO
1000
100OJ
100
toooo
100
100
too
10000
AOO
100
too
100
100 '
100
100
100
1000
reparation
SpikofuL)
Fvol(100mL)
5000
5000
5000
950
5000
sooo
6000
5000
950
5000
SOOO
5000
5000
scco
9SD
SCCO
tsoo
sx»
aso
5000
5000
axe
1S60
5003
5000
SOOO
SCCO
5000
SCCO
5000
5000
1500
cone
(Pf>m)
5
5
5
95
5
S
S
5
95
S
5
S
5
5
95
50 '
ISO
S
ss
5
5
S
195
6
5
S
5
S
5
5
5
15
SPIKING
ram Spitting Standard
>ptke(uL) cone
^VolOOOml)
1000
1000
1000
1000
1000
1000
1000
1000
1000
1000
1000
1000
1000
1000
1CCO
1000
toco
1000
(000
1000
TOOO
toco
1000
1000
1000
1000
1000
1000
1000
1000
1000
1000
(PPO)
50
50
50
960
50
50
so
so
950
so
50
SO
50
SO
950
|_ 500
1500
50
560
SO
50
SO
1950
SO
50
SO
50
SO
SO
50
50
150
combined
total
1000
1000 |
1000
200O
tooo
2000
SCO
**SpikB aapoiataly
Etemont Orig Std
Au
Ca
Li
P
Pd
Pt
S
a
Sn
Sf
1000
1000 •
1000
1000 -
1000
1000
1000
10000
1000
1000
140
30
70
100
160
300
350
SO
20
S
""—' -
- 1400 •:-
-300 -
— TOO '
•• .1000 -
1600 ••
3000 -
• 3500 •»
SOOO
200
SO
• 3^*3y*
1000UL or ma Spiking Standard gives tfia tetad cone, of ma abova atemanto.
SpHeJng Standard 3-62-1
EXP: 10/28/98
Spiked by:
Pradigeotiorv
PostoigaGuon-
-------
PAGE 1 OF 1
TRIANGLE LABORATORIES, INC.
Transfer Chain-of-Custody Form
Project 46705-A
Transfer From: IWL To: IA I
Initials. . Date Time. . .
Released by: y/jyvy- \ /^^/^^"^
.*. / i
P- ^S"
{*-***:_ -^—.'
Accepted by:
MILES. ID TLI No,
Cust.Id.
46705-A -000 TLI Blank
46705-A -001 218-12-1
46705-A -002 218-12-2
46705-A -003 218-12-5
46705-A -004 218-12-8
46705-A -005 218-12-3
46705-A -006 218-12-6
46705-A -007 218-12-9
46705-A -008 LCS
46705-A -009 218-12-1 D
46705-A -010 218-12-3 MS
46705-A -Oil 218-12-3 MSD
TLI Blank
AC1B
AC2B
AC3B
AC4B
RAP2B/AC
RAP3M2/AC
RAP5B/AC
LAB CONTROL SPIKE
AC1B DUPLICATE
AC3B MATRIX SPIKE
AC3B MATRIX SPIKE DUP.
Additional comments or instructions
-XfrCOC (Rev 11/01/94)--
37
-------
SEE SPIKE LOG
Projert * '
EXPdata
en/99
8/1/99
6/1/99
e/i/99
en/99
en/99
en/99
e/i/99
en/99
B/1/99
e/i/99
en/93
8/1/99
en/ss
en/99
en/99
8/1/33
en/as
S/1/99
en/99
3/1 /»
e/1/aa
en ,-99
an/99
en/99
an/99
SpMcfrig Standard Preparation
Element Standard Ortg. Std. Spika(uL) cone
ID (ppm)
^9
Ko
U
M
3
3a
fe
^a
;a
Id
;o
;r
:u
:«
r«
K
(
*g
Kg
*n
Me
-la 1
»a
4i
»S
Sb
E»
T
n
/
In
!n
a«4-7
3«O8
3«4-7
a«>6
3-54-7
»54-7
3-6CX8
3«oe
3^0-10
&33-S
3«W
»6CW
3«>e
3*00
3-6O9
3*4-7
3^5-5
39
»«W
3^4-7
a^o^-?^
3-eo-e
o-eo-9
3-ea<
!i«i-e
3««
3«M3
3^0-5
3-5O9
«O-7
100
100
100
10000
100
100
100
100
10000
100
100
100
100
100
10000
1CCO
10CXC
ICO
' TOOX7
ICO
IOC?
ICC
10000
1CO
100
10C
100
100
100
100
100
1000
FvoldOOmL) (PP™)
5000
sooo
scoo
950
scoo
5000
sooo
sooo
960
sooo
sooo
sooo
scoo
5CCO
950
5CCO
TS07
5000
5
5
S
96
5
5
5
S
95
S
5
5
S
5
as
so
rsj
5
5*0 ( SS
50CO I 5
5000
sccc
1S50
5000
seco
sex
5CCO
scoo
5000
soco
50CO
1500
5
e
JS5
5
5
S
S
S
S
S
5
15
SPIKING
'mm Spiking Standard
3pika(uL) cone
=Vol{100ml)
1000
1000
1000
1000
1000
1000
1000
1000
1000
1000
1000
10CO
1000
1COO
1000
10CO
1033
1CCO
TOCO
10CO
IOOO
1000
1000
1000
;oco
tooo
1000
1000
1CCO
1000
1CCO
1000
(PPb)
so
so
so
960
so
50
so
50
950
so
so
so
50
50
aso
SCO
tax?
so
dSO
so
50
5C
>9SO
50
50
so
so
so
50
50
50
150
combined
total
1000
1CCO
1000
2003
TOOO
2000
200
"Spike separately
Element Orig Std
(PP<")
Spika(uL) cone
FvolflOOm (ppb)
Au
C«
U
p
Pd
Pt
S
SI
Sn
Sr
1000
1000
1000
1000
1000
1000
[_ 1000
10000
1000
1000
140
30
70
100
160
300
360
SO
20
S
1400
300
700
1000
1600
3000
3500
SOOO
200
50
ICOCuL of tfia Spiking Standard fjrveo tfta listed cone, of :.la abova atomanto.
Spiking Standard 3-62-2
EXP: 10/28/98
Spiked by:
Poateiigeation-
38
-------
, . /aJraf*
£
m
''
^r Pc"£-iw-ci^. ^lt?*^X^r
3£fifee&£!5 'FfrfcnFi?
i. *K -^i/i* ^^
-------
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13 O
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-
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"
>
-------
PAGE 1 OP 1
Project: 46705A
TRIANGLE LABORATORIES, INC. |
Sample Preparation Tracking & Management Form |
Client: Pacific Environmental Services (PES03) I
Solvent/Acids 0 :
REV 07/26/93 (PSTMF 7)--+
41
-------
PAGE
MERCURY SPIKE LOG
PROJECT #
SAMPLE IDs
J&L
ORIGINAL
SPIKE
CONC. (Hg)
0* Ij
STANDARD #
WORKING
STANDARD
PREPARED
FROM
SPIKE
AMOUNT
(mL)
5-
SPIKE
SAMPLE
(PPB)
INITIALS
WfTNES
r
iforms\hgspke.log (08/22/96)
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r= • - o «r>
• a --« -=- zt
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r "j -Zi
'J. i~»
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feat File: EG..HL '=
lent: Eg
it Data: Hain+Snppl.
it; Califa. Carve
arks:
AiOAEOS: SPKI 3-70-6,g-
: HIGS PORITY 3-70-5,7
TROHEiT: 5100
eleigth: 253.7 Peak
lal Type: Ai
1 Tiie: 30.0
)le Replicates: 1
idard Replicates: 1
le Type: Air
!ait Flos: 10.0 L/iin
Analyst: EDIAEDS
Peak Storage: Jpne
Technique: US ?ersioi: 7.01
Slit: 0.70 Lo»
Signal Keasireiett: Peal Height (5)
Read Delay: 0.5 HOC Tiie: 2
Plate Sensor: OB
Fael Floi: 2.0 L/iit
BEAT [OS:
utious ', ID
i
L 01, .I. 10*11 HT7
D. olauK |31U DL&
dard 1 ,'STD 1
dard 2 ,'STD 2
iard 3 ,'STD 3
lard * ,'STD 4
lard 5 |STD 5
iard 8 1STD S
ibration Qnits: og/L
ibration Type: Liiear
Cone
0.200
0.500
1.000
J.OOO
5.000
10.000
Saipl
j
>. Oiits: ag/L
.z Check Calculations:
'fereice for Dupls: So Locations:
;o»ery for Spike: So Locations:
Cone:
73
-------
CD <»
•• •• » « ^ ?s {
4D oa rs» «—. i
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*- >. pea 50 «A •* i
^B c/a «-o oo i
PB1 «=» «*• f3^ I
« CO * I
B ^S
-------
lent File: IG .ML ' Eleient: Bg lavelength: 253.7
e: 09/22/98 liie: 14:34 Slit: Q.70 I
a Pile: AB936.DAT IB/It file: AB936.IDI" lap Current: 0
hniqne: KBS Calib. Type: linear Energy: 75
ark 1: STABDARDS: SPEI 3-70-6,8
ark 2: QC: HIGH PORITT 3-70-5,7
ID: STD BLiU Se<. Ho.: 00037 A/S Poa.: - Date: 09/22/98
licate 1 Tiie: 14:35
i Area (A-s): -0.019 Peak Height (A): 0.000
ik Corrected Pk Height (A): 0.000
:entration (ug/L ): 0.000
i-zero perfoned.
ID: STDl=0,2ag/L Seq. lo.: 00038 A/S PCS.: -- Date: 09/22/98
icate 1 Tiie: 14:35
Area (A-s): 0.056 Peak Beight (A): 0^004
k Corrected Pk Height (A): 0.004
entration (ag/l ): 0.058
dard mber 1 applied. [0.200]
ilation coefficient: 1.00000 Slope: 0.0196
ID: STD2:0.5ag/l Seq. So,:
A/S Pos.: -- Date: 09/22/9H
[e abs. is greater than that of the largest standard.
.cate 1 Tiie: 14:37
Area (A-s): 0.259 Peak Height (A): 0.016
: Corrected Pk Height (A): 0.016
'.ntration (ug/L ): 0.795
ard nuiber I applied. (0.500!
latioi coefficient: 0.94072 Slope: 0.0300
ID: STDJst.Qij/l Seq. Ho.:
A/S Pos.: -- Date: 09/22/98
e abs. is greater thai that of the largest standard.
cate 1 Tiie: 14:38
Area (A-s): 0.605 Peak Height (A): 0.036
Corrected Pk Height (A): 0.038
atration (ag/L ): 1.189
ird nmber 3 applied. [1.000]
lation coefficient: 0.98278 Slope: 0.0346
ID: STD4=2.Qag/l Seq. Jo.:
A/S Pog.: - Date: 09/22/91;
' abs. is greater than that of the largest standard.
ate 1 Tiie: 14:39
rea iA-s|: 1.235 Peak Height (A): 0.072
75
-------
Blank Corrected Pk Beight (Aj: 0.072
Concentration (ig/L ): 2.084
Standard amber 4 applied. [2.000] -
Correlation coefficient: 0.99658 Slope: 0.035?
ig ID: STD5=5.0ig/l Seq. So,:
A/S Pos.: -"- Date: 09/22/98
Saiple abs. is greater that that of the largest standard.
Replicate 1 Tiie: 14:40
Peak Area (A-s|: 3.HO Peak Eeight (A): 0.199
Blank Corrected Pk Eeight (A): 0.198
Concentration (ng/l ): 5.532
Standard nuiber 5 applied. [5.000]
Correlation coefficient: 0.99820 Slope: 0.0389
Saiple abs. is
Replicate 1
Peak Area (A-s)
Blank Corrected
Concentration
Standard
Corr
3g ID: STD6=10.Qng/l Seq. So.: 000(4 A/S Pos.: -- Date: 09/22/98
Saipie abs. is greater than that of the largest standard.
Replicate 1 Tiie: 14:48
Peak Area (A-s): 6.321 Peak Eeight (A): 0.389
Blank Corrected Pk Eeight (A): 0.389
Concentration (ug/l ): 11.673
Standard amber 6 applied. [10.0001
Jorrelatioc coefficient: 0.99952 Slope: 0.0389
71
-------
lent File: HG .KZL
:: 09/22/98
i Pile: AB936.DAT
miqae: KBS
Kleieit: Hg
file: 14:«
ID/It File: AB936.IDI
Calib. Type: Linear
hreleigth: 253.7
Slit: 0.70 I
Laip Current: 0
Energy: 75
irk 1: STAiDARDS: SPKI 3-71-6,8
irk 2: QC: IICI PDR1TY 3-70-5,7
M
Display Calibration - C:\flflJJSER\flflJILES\ELEHENT\H6_.MEL
9.389,
S4
JS5
Linear
Corn. Coef.: B.99962
Slope: 0,0389
Concentration
18.800
ID: !CV=Ung/L
caw 1
Seq. So.: 000(5 A/S Pos.: -- Date: Q9m/9F
Tiie: 14:51
Arei lA-sj: 2.327 Peak leight (A): G.U1
, Corrected Pk Height (A): 0.141
ntratioa lug- I ): 3.638
ID: ICB
Seq. So.: 00045 A/S Pos.
cue 1
4m (4-sl: -0.118
Corrected Pk Jeight (A): -O.I
untie* ing/1 ): -0.124 •
Tiie: 14:53
Peak Height (A):
ID: CHECE LC
Seq. So.:
A/S Pos.
:ate 1
irea(A-s): 0.009
Corrected Pk Height (A): Q.303
itritioi (ag/L ): 0.033
Tiie: 14:54
Peak Height (A):
Date: 09/22/9F
Date: 09/22/9F
77
-------
.eient File: EG .MEL Eleient: Eg taielength: 253.7
ite: 09/22/98 Tiie: 15:22 Slit: 0.70 L
ita File: AB936.DAT ID/It File: AB936.IDS Lup Current: 0
echnique: MHS Calib. Type: Linear Energy: 75
eiark 1: STABDABDS: SPEI 3-70-6,8
eiark 2: «C: EIGB PURITY 3-70-5,7
I ID: 46705A MB Seq. 80.: 00068 A/S Pos.: -- Date: 09/22/9?
epiicate 1 Tiie: 15:23
eak Area (A-s): 0.016 Peak Eeight (A): 0.002
>.:k Corrected Pk Beight (A): 0.002
-.eatration (ug/L ): 0.041
g ID: 46705A MBD Seq. 80.: 00069 A/S Pos.: - Date: 09/22/9?
epiicate 1 Tiie: 15:24
eak Area (A-s): 0.011 Peak Eeight (A): -0.000
lank Corrected Pk Height (A): -0.000
oncentratioi (ug/L ): -0.003
g ID: 46705A LCS Seq. So.: 00070 A/S Pos.: - Date: 09/22/9?
.epiicate 1 Tiie: 15:25
•eak Area (A-s): 2.871 Peak Eeight (A): 0.170
>lank Corrected Pk Beight (A): 0.170
Concentration (ug/L I: 4.384
:g ID: 46705A LCSD Seq. Bo.: 00071 A/S Pos.: - Date: 09/22/9?
ieplicate 1 Tiie: 15:26
'eak Area (A-s): 2.853 Peak Eeight (A): 0.164
Blank Corrected Pk Beight (A): 0.164
Concentration (ug/L ): 4.219
It ID: 218-12-1 Seq. So.: 00072 A/S Pos.: -- Date: 09/22/9?
Jeplicate 1 Tiie: 15:27
Peak Area (A-s): -0.002 Peak Eeight (A): -0.001
Blank Corrected Pk Height (A): -0.001
Concentration Ug/L ): -0.018
Eg ID: 218-12-1 D Seq. io.: 00073 A/S Pos.: - Date: 09/22/98
Seplicate 1 Tiie: 15:28
Peak Area (A-s): 0.017 Peak Eeight (A): 0.000
Blank Corrected Pk Height (A): Q.QOO
Concentration (ug/L ): 0.010
Eg ID: 218-12-3 Seq. Io.: 00074 A/S Pos.: - Date: 09/22/9?
78
-------
ate 1 Tiie: 15:29
rea (A-s): -0.02* Peak Height (A): -0,001
Corrected Pk Height (A): -0.001
tratioa (ug/l |: -0.034
ID: 218-12-3 D Seq, So.: 00075 A/S Pos.: -- Date: 09/22/98
:ate 1 Tiie: 15:30
lfea(A-s!: -0.025 Peak Height (A): -0.001
Corrected Pk Height (A): -0.001
itration (ag/l ): -0.028
ID: 218-12-3 KS Seq. So.: 00076 A/S Pos.: -- Date: 09/22/9S
:ate 1 Tiie: 15:33
Irea (A-s|: 2.638 Peak Height (A): 0.152
Corrected Pk Height (A): 0.152
itratioi Ug/L ): 3.915
ID: 218-12-3 USD Seq. So.: 00077 A/S Pos.: -- Date: 09/22/9P
cate 1 Tiie: 15:31
Area (A-s): 2.7*0 Peak Height (A): 0.168
Corrected Pk Height (A): 0.168
atration (ug/l ): (.330
ID: CCVl=6.0ug/l Seq. So.: 00078 A/S Pos.: -- Date: 09/22/98
cate 1 Tiie: 15:35
Area lA-s): 3.431 Peak Height (A): 0.220
•.Corrected Pk Height (A): 0.220
sutratioa (ug/L ): 5.654
ID: CCB Seq. So.: 00079 A/S Pos.: -- Date: 09/22/98
icate 1 Tiie: 15:36
Area (A-s): -0.075 Peak Height (A): -0.003
k Corrected Pk Height (A): -0.003
entratiot (ug/L ): -0.065
ID: 218-12-2 Seq. So.: 00080 A/S Pos.: -- Date: 09/22/98
icate 1 Tiie: 15:37
Area (A-s): -0.048 Peak Height (A): -0.001
k Corrected Pk Height (A): -0,001
eatratioa Ug/L ): -0.028
ID: 218-12-2 D Seq. So.: 00081 A/S Pos.: - Date: 09/22/98
icate 1 Tiie: 15:41
Area (A-s): -0.049 Peak Height (A): -0.002
ik Corrected Pk Height I A): -0.002
79
-------
oaceatratioa (ug/l ): -0.041
i ID: 218-12-5 Seq. 80.: 00082 A/S Pos.: -- Date: 09/22/9P
.eplicate 1 Tiie: 15:47
eak Area (A-sj: -0.040 Peak Height (A): -0.001
ilaak Corrected Pk Height (A): -0.001
loaceatratioa ing/1 ): -0.013 -
ig ID: 218-12-5 D Seq. Ho.: 00083 A/S Pos.: -- Date: 09/22/98
lepiicate 1 Tiie: 15:48
3eak Area (A-sl: -0.036 Peak Height (A): -0,000
Uaak Corrected Pk Beight (A): -0.000
loaceatratioa Ug/L ): -0,005
ig ID: 218-12-8 Seq. So.: 00084 A/S Pos.: -- Date: 09/22/98
ieplicate 1 Tiie: 15:49
Jeak Area (A-s|: -0.03? Peak Height (A): -0.001
Blank Corrected Pk Height (A): -0.001
:oaceatratioa lug/L ): -0.018
It ID: 218-12-8 D Seq. So.: 00085 A/S Pos.: -- Date: 09/22/9F
Jeplicate 1 Tiie: 15:50
Peak Area (A-s): -0.050 Peak Height (A): -0.001
Blaak Corrected Pk Height (A): -0.001
^oaceatratioa (ug/L I: -0.034
3g ID: 218-12-6 Seq. So.: 00086 A/S Pos.: -- Date: 09/22/98
Jepiicate 1 Tiie: 15:51
Peak Area |A-s': -0.064 Peak Height (A): -0.002
Eiaak Corrected Pk Height (A): -0.002
Concentmioa iug/l ): -0.049
Sg ID: 218-12-6 D Seq. So.: 0008? A/S Pos.: -- Date: 09/22/98
Jeplicate 1 Tiie: 15:52
Peak Area (A-s): -0.059 Peak Height (A): -0.002
Blaak Corrected Pk Height (A): -0.002
Coaceatratioa (ag/L ): -0.044
Hg ID: 218-12-9 Seq. lo.: 00088 A/S Pos.: -- Date: 09/22/98
Beplicate 1 Tiie: 15:53
Peak Area (A-s): -0.057 Peak Height (A): -0.002
Blaak Corrected Pk Height (A): -0.002
Concentration (ag/l ): -0.039
80
-------
ID: 218-12-9 D
Seq. Ho.:
A/S Pos.
Date: 09/22/98
iplicate 1
lak Area (A-s): -0.066
lank Corrected Pk Height (A): -O.
mcentratioa (ug/L ): -0.052
Tiie: 15:55
Peak Height (A):
Tiie: 15:58
Peak Height (A): 0.179
! ID: CCV2=Uug/L Seq. Bo.:
iplicate 1
;ak Area (A-sl: 3,080
;ink Corrected Pk Height (A): 0.194
incentration (ug/L I: 4.996
A/S Pos.: -- Date: 09/22/9?
Tiie: 16:02
Peak Height (A): 0.194
ID: CCB
Seq. Ho.:
A/S Pos.:-- Date: Q9/22/9P
jplicate 1
;ak Area (A-si: -Q.060
lank Corrected Pk Height (A): -0.0
jacentration (ug/L I: -0.057
Tiie: 16:03
Peak Height (A): -0.0
81
-------
CASE NARRATIVE
Analysis of Samples for the Presence of Trace Metals
Methods
6010A
7000A Series
7470
Rev.l (7/92)
Rev.l (7/92)
Rev.O (9/86)
Client:
TLI Project Number:
Date:
Pacific Environmental Services
46705B
September 23, 1998
This report should only be reproduced in full.
renroduction of this report requires permission
Triangle Laboratories, Inc.
Rev. 25-Sep-96
Triangle Laboratories, Inc.
801 Cap/to/a Drive P.O. Box 13485
Durham, NC 27713-4411 Research Triangle Park, NC 27709-3485
919-544-5729 Fax # 919-544-5491
-------
Triangle Laboratories, Inc. September 23,1998
Case Narrative TLI Project #: 46705B
Overview
Three aggregate samples were analyzed for arsenic (As), beryllium (Be), cadmium
(Cd), cobalt (Co), chromium (Cr), manganese (Mn), nickel (Ni), lead (Pb), antimony
(Sb), selenium (Se), and mercury (Hg). For all analyses (except Hg), the samples and
associated QC samples were prepared by hotplate digestion following the guidelines of
EPA SW-846 Method 3050A. The samples and associated QC samples for the analysis
of Hg were prepared following the guidelines of EPA SW-846 Method 7471 Rev.O
(9/86). The samples were analyzed following the guidelines of EPA SW-846 Methods
6010A Rev. 1 (7/92), 7471 Rev. 0 (9/86), and 7000A Rev. 1 (7/92) series. Results
reported relate only to the items tested.
OC Remarks
The release of this set of data by Triangle Laboratories, Inc. was authorized by the
Quality Control Chemist who has reviewed each sample data package individually
following a series of inspections/reviews. When applicable, general deviations from
acceptable QC requirements are identified below and comments are made on the effects
of these deviations upon the validity and reliability of the results. Specific QC issues
associated with this particular project are:
Sample Receipt:
i - .. ,C ,s, v 11
Three aggregate samples, four liquid AC and three asphalt cement samples were received
at 25 °C on September 15, 1998 in good condition. These samples were received in a box
instead of a cooler.
Sample Preparation:
Laboratory documentation of the sample preparation is included in the data package.
Instrumentation:
Arsenic (As), beryllium (Be), cadmium (Cd), cobalt (Co), chromium (Cr), manganese
(Mn), nickel (Ni), lead (Pb), antimony (Sb), selenium (Se), concentrations were
determined by Inductively Coupled Plasma Emission Spectroscopy (ICP).
Beryllium (Be) concentrations for the front half samples were analyzed by Graphite
Furnace Atomic Absorption (GFAA).
Mercury (Hg) concentrations were determined by Cold Vapor Atomic Absorption
(CVAA).
The linear range for the instrument TJA 61E Trace Analyzer was based on four
standards and a blank, which established a correlation coefficient value greater than or
-------
Triangle Laboratories, Inc. September 23, 1998
Case Narrative TLI Project #: 46705B
equal to 0.995. A calibration curve, based on a blank and one standard, is established
for each analytical run, followed by a check high standard and an initial calibration
verification (ICV). The check high standard does not deviate from the calibration
curve by more than 5 % . In addition, continuing calibration verifications (CCVs) are
performed throughout the analytical run.
A Reporting Detection Limit (RDL) is used instead of an Instrument Detection Limit
(IDL). The spectrometer and atomic absorption instruments can achieve low detection
limits between 0.2-8 ppb levels for many analytes. Triangle Labs is using RDL values
of 1-10 times the IDL as detection limits for reporting purposes.
Data Review:
All analytes found hi the method blank (MB) are detected at a level equal to or less
than the respective Reporting Detection Limit (RDL).
The sample results are based on dry weight.
A sampling date was not supplied by the client and the sampling to analysis holding
tunes cannot be determined. All samples were analyzed within 7 days of sample
receipt at Triangle Laboratories.
The pre-digestion spike (MS) and the pre-digestion spike duplicate (MSD) for Sb, also
the pre-digestion spike duplicate (MSD) for Pb for the sample RAP5B/AGG
demonstrated percent recoveries outside the QC criteria which may indicate significant
matrix effects specific to these analytes in the native sample matrix. Please note that
the post-digestion spike (PDS) met QC criteria for Sb and Pb for sample RAP5B/AGG.
Also note the the results for Sb hi this sample should be considered biased low due to
matrix interferences.
The recoveries for the matrix spike (MS), matrix spike duplicate (MSD), and post-
digestion spike (PDS) are not reported for Mn and Pb for the sample RAP5B/AGG.
The spike concentrations added were insignificant in comparison to the levels of these
analytes present hi the native sample. ,
• • •• • ' • i N . : . . -
The duplicate analyses for Cr and Ni for the sample RAP5B/AGG demonstrated RPDs
outside the QC criteria of 20.0 percent, which indicates the presence of a significant
amount of interferents specific to these analytes hi the native sample matrix.
The post-digestion spike (PDS) for Be for sample RAP5B/AGG demonstrated a percent
recovery outside the QC criteria of 80-120 percent, which indicates significant matrix
effects specific to this analyte hi the native sample matrix. The interference QC
analysis is not reported (i.e. PDS, MS, MSD, and serial dilution) for this analyte since
the Method of Standard Additions (MSA) was performed. The MSA results are
3
-------
Triangle Laboratories, Inc. September 23,1998
Case Narrative TLI Project #: 46705B
The post-digestion spike (PDS) for Be for sample RAP5B/AGG demonstrated a percent
recovery outside the QC criteria of 80-120 percent, which indicates significant matrix
effects specific to this analyte in the native sample matrix. The interference QC
analysis is not reported (i.e. PDS, MS, MSD, and serial dilution) for this analyte since
the Method of Standard Additions (MSA) was performed. The MSA results are
reported if the correlation coefficient value is at least 0.995. The MSA results are
reported for all samples.
QC requirements:
The analytical duplicates for analytes analyzed by GFAA cannot be considered valid
qualifiers if the concentrations of the analytes in the original and/or duplicate sample
are not at least five times the respective RDL. The RPDs for these analyses are
indicated by "
-------
Triangle Laboratories, Inc. September 23,1998
Case Narrative TLI Project #: 46705B
The quality control range for percent recoveries of post-digestion spiked samples
analyzed by ICP is 75-125. If recoveries are outside this range, a matrix effect is
suspected.
The quality control range for percent recoveries of spiked samples analyzed by CVAA
is 75-125. If recoveries are outside this range, a matrix effect is suspected.
If the analyte concentrations analyzed by GFAA in the native samples are less than five
times the respective RDLs, or if valid serial dilution analyses demonstrate RPDs
outside the ten percent quality control range, the percent recoveries of post-digestion
spiked samples is 85-115. If recoveries are outside this range, all matrix-related
samples are analyzed by the Method of Standard Additions (MSA). The MSA analysis
for each sample is reported only if the correlation coefficient value is at least 0.995.
By our interpretation, the analytical data in this project are valid based on the
guidelines of US EPA SW-846 Methods 6010A Rev. 1(7/92), 7000A Rev. 1 (7/92)
series, and 7471 (9/86). Any specific QC concerns or problems have been discussed hi
the QC REMARKS section with emphasis on their effect on the data. Should Pacific
Environmental Services have any questions or comments regarding this data package,
please feel free to contact Triangle Laboratories, Inc., at (919) 544-5729.
For Triangle Laboratories, Inc.,
Report Preparation Quality Control
Brenda W. Bell Leslie D. Jones
Report Preparation Chemist Report Preparation Chemist
The total number of pages in this data package is:
-------
TRIANGLE LABORATORIES, INC
LIST OF CERTIFICATIONS AND ACCREDITATIONS
ENVIRONMENTAL
American Association for Laboratory Accreditation. Accredidation pending. Certificate
Number 0226-01. Accreditation for technical competence in Environmental Testing. (Including
Waste Water, Sol/Haz Waste, Pulp/Paper, and Air Matrices) Parameters are AOX/TOX, and
Dioxin/Furan. Method 1613 for Drinking Water Currently re-applying..
State of Alabama, Department of Environmental Management. Expires December 31, 1998.
Laboratory ID. # 40950. Dioxin in drinking water.
State of Alaska, Department of Environmental Conservation. Expires December 21, 1998.
Certificate number OS-006-98. Dioxin in drinking water.
State of Arizona, Department of Health Services. Expires May 26, 1998. Certificate
#AZ0423. Drinking Water for Dioxin, Dioxin in WW and S/H Waste. Currently appying for
renewal.
•
State of Arkansas, Department of Pollution Control and Ecology. Expires February 19,
1999. Pulp/paper, soil, water, and Hazardous Waste for Dioxin/Furan; AOX/TOX, Volatiles,
Semi-volatiles, and Metals.
State of California, Department of Health Services. Expires August 31, 1999. Certificate
#1922. Selected Metals in Waste Water, Volatiles, Semi-volatiles, and Dioxin/furan in WW and
Sol/Haz Waste. Dioxin in drinking water.
State of Connecticut, Department of Health Services. Expires September 30,1999.
Registration #PH-0117. Dioxin in drinking water.
Delaware Health and Social Services. Expires December 31,1998. Certificate #NC 140.
Dioxin in drinking water.
Florida Department of Health and Rehabilitative Services. Expires June 30,1998. Dioxin in
SDW. Drinking Water ID HRS# 87424. Pending new certificate.
Triangle Laboratories, Inc.
801 Capitola Drive P.O. Box 13485
^ ... . "... . Durham, NC27713-4411 Research Triangle Park,-N&27709-348
y:certific\certJistmem 919-544-5729 Fax#9i9-S44-549i _.
-------
Hawaii Department of Health. Expires March 1, 1999. Dioxin in drinking water. "Accepted"
status for regulatory purposes.
Idaho Department of Health and Welfare. Expires December 31,1998. Dioxin in drinking
water.
State of Kansas, Department of Health and Environment. Expires January 31, 1999.
Method 1613 for drinking water. ED #'s - Drinking water and/or pollution control - E-10215.
Solid or Hazardous Waste - E-101209.
Commonwealth of Kentucky, Department for Environmental Protection.
Expires December 31,1998. ID#90060. Dioxin in drinking water.
Maryland Department of Health and Mental Hygiene. Expires September 30, 1998.
Certification #235 Drinking water by Method 1613 A. Currently applying for renewal.
State of Michigan, Department of Public Health. Expires June 30, 1999. Drinking water by
Method 1613. Current certification is extended, based on New York certificate renewal.
Mississippi State Department of Health. No expiration date. Dioxin in drinking water.
Montana Department of Health and Environmental Services. Expires December 31, 1998.
Dioxin in drinking water. '
State of New Jersey, Department of Environmental Protection and Energy. Expires June 30,
1998. Extended until July 31, 1998 per letter dated May 29, 1998. ID #67851. BNAs and
Volatiles. Dioxin in drinking water. Currently applying for renewal.
State of New Mexico, Environment Department. Still certified, awaiting information from
A2LA Dioxin in drinking water.
New York State Department of Health. Received updated certificates. ED #11026.
Environmental Analyses of potable water, non-potable Water, Solid and Hazardous Waste.
Method 1613 in DW.
State of North Carolina, Department of Environment Health and Natural Resources
Expires. August 31,1998. Certificate # 37751. Dioxin in drinking water.
State of North Carolina, Department of Environment, Health, and Natural Resources,
Division of Environmental Management Expires December 31,2000. Certificate # 485.
Metals, pesticides & PCBs, semi-volatiles and volatiles; TCLP.
R«vis«d 8/3/98
-------
North Dakota State Department of Health and Consolidated Laboratories. Expires
December 31,1998. Certificate # R-076. Effective October 4,1993. Dioxin in drinking water.
Oklahoma Department of Environmental Quality. Expires August 31, 1998. Laboratory
#9612. Dioxin by 1613A, 8290 and 8280. Submitted renewal application 7/1.
State of South Carolina, Department of Health and Environmental Control. Expires
June 30, 1998. Extended August 31, 1999. Certificate number #99040001 (drinking water).
Expires August 31, 1999. Certificate number #99040002 (other parameters). Dioxin/Furans,
BNA, Volatiles, and PCBs/pesticides under Clean Water Act, 2,3,7,8-TCDD for Drinking Water,
and Organic extractables for Solid and Hazardous Waste.
State of Tennessee. Department of Environment and Conservation. Expires
February 5, 1999. ID #02992. Method 1613 Drinking water only.
U.S. Department of Agriculture Soil Permit Expires September 30, 2001. Permit No. S-
3790. Under the authority of the Federal Plant Pest Act, permission is granted to receive foreign
soil samples for use in laboratory analysis.
U.S. Army Corps of Engineers. Expires October 19, 1999. Validated to perform analyses for
the Fort Belvoir, VA (Contract Number DACA31-97-D-0029), Vint Hill Farms Station, Vint Hill,
VA (Contract Number DACA31-95-D-0083), and Selma Pressure Treating Superfund Site,
Selma, CA (Contract number DACW45-94-D-0054).
U.S. EPA Region V. Expires November 14, 1999. Dioxin in drinking water.
U.S. EPA Region VTH, for the State of Wyoming. Expires November 12, 1998 Dioxin in
drinking water.
State of Utah, Department of Health. Expires May 30,2000. Certificate Number E-166.
Certification for the following parameters: Semi-Volatiles and Volatiles under RCRA; Volatiles
under Clean Water Act; DioxinVfiirans by Method 8280; Drinking water for Dioxin by Method
1613; Metals including Mercury and Microwave Digestion.
Commonwealth of Virginia, Department of General Services, Division of Consolidated
Laboratory Services. Expires June 30, 1999. ID #00341. Dioxin in drinking water.
State of Washington, Department of Ecology. Expires September 11,1998. Lab
Accreditation Number C067. Scope of Accreditation applies to water analyses for
y:certific\certlist.mem
-------
Polychlorinated Dibenzo-p-dioxins and Polychlorinated Dibenzofurans, BNA Extr (Semivolatile)
Organics and Purgeable (Volatile) Organics.
State of Washington, Department of Health. Expires April 30, 1999. Dioxin in drinking
water. Lab I.D. 129.
State of West Virginia, Department of Health. Expires December 31, 1998. Certificate No.
9923(C). Dioxin in drinking water.
State of Wisconsin, Department of Natural Resources. Expires August 31, 1998. Laboratory
ED Number 999869530. Certification for the following categories of Organics: Purgeable,
Base/Neutral, Acid, PCBs, and Dioxin. Expires November 14, 1999. Laboratory ED 999869530.
Dioxin in drinking water.
PHARMACEUTICAL
Drug Enforcement Agency (DEA). Expires November 30, 1998. Registration number
RT01195835. Controlled substance registration for schedules 1,2,3,3N,4,5.
N.C. Department of Human Resources. Expires October 31, 1998. Registration number
NC-PT 0000 0031. North Carolina controlled substances registration. Application submitted for
renewal.
Food & Drug Administration (FDA) Registration. Expires June 1998. ID #'s 001500
1053481. Annual registration of drug establishment.
OTHER
Clinical Laboratory Improvement Amendments (CLIA) Registration. Expires May 30,
1999. DD#34D0705123. Department of Health & Human Services, Health Care Financing
Administration.
U.S. EPA Large Quantity Hazardous Waste Generator. No expiration date. EPA ED
#NCD982156879. Permit indicates that the laboratory is a large generator of hazardous waste.
North Carolina General License for Radiation Protection. No expiration date. No License.
032-875-OG. The general license applies only to radioactive material contained in devices which
have been manufactured and labeled in accordance with specific requirements.
IfeviMd 8/3/98
-------
DOCUMENT
CONTROL
MlCapftofe OHM* RO. Box 13495
OU/IAIIL MC 2771&4£11 AMMHGV 77BDS
919*444729 ft* * 919*4+9491
r ' in
-------
f PACIFIC ENVIRONMENTAL SERVICES, INC.
Central Park West
5001 South Miami Boulevard, P.O. Box 12077
Research Triangle Park, North Carolina 27709-2077
(919) 941-0333 FAX: (919) 941-0234
Sample Chain Of Custody Record
PLANT: US EPA HOT MIX ASPHALT PLANT C
RECOVERY PERSON: J. Swift
PROJECT NO.: S508.001
SAMPLERS: N/A
Sample
ID
AC1B
AC2B
RAP2B/AC
RAP2B/AGG
AC3B
RAP3M2/A
KAP3M2/*
C
fc(*
AC4B '
RAP5B/KC
RAP5B //\&G
Sample
Name
Liquid AC, Run 1 Begin
Liquid AC, Run 2 Begin
Recycled Asph, Run 2 Begin (Asphalt Cement)
Recycled Aspji, Run 2 BeginJAggregate)
Liquid AC, Run 3 Begin
Recycled Asph Run 3 Middle (Asphalt Cement)
Recycled Asph Run 3 Middle (Aggregate)
Liquid AC, Run 4 Begin
Recycled Asph, Run 5 Begin (Asphalt Cement)
Recycled Asph, Run 5 Begin (Aggregate)
No.
of
Cont.
1
1
1
V
1
1
1
1
1
1
Relinquished by:
fr\^2SH/ViA_ C&NNOO/
Relinquished by:
Analytical Request
Metals* using 7000 series (SW-846)
Metals* using 7000 series (SW-846)
Metals* usii»a 6010/7000 series (SW-B46^
Metals* using 6010/7000 series (SW-846)
Metals* using 7000 series (SW-846)
Metals* using 6010/7000 series (SW-846)
Metals* using 6010/7000 series (SW-846)
Melals* using 7000 series (SW-846)
Metals* using 6010/7000 series (SW-84G)
Melals* using 6010/7000 series (SW-846)
Comments
* 11-Sb, As, Be, Cd, Cr, Pb, Mn, Ni. Se, Co,& Hg
* 11-Sb, As, Be, Cd. Cr, Pb, Mn, Ni, Se, Co.&jjg
* 11-Sb, As, Be, Cd, Cr, Pb, Mn. Ni, SeLCo,& I Ig
* 11-Sb, As, BeLCd, Cr, Pb, Mn, Ni. Se, Co,& Hg
* 11-SbLAs, Be, Cd, Cr. Pb^Mn, Ni, Se, Co..', I U|
* 11-Sb. As, Be. Cd, Cr, Pb, Mn, Ni, Se, Co.& Hg
* 11-Sb, As, Be. Cd. Cr, Pb, Mn, Ni, Se, Co/, 1 Ig
* 11-Sb. As, Be, Cd, Cr, Pb, Mn, Ni, Se, Co,& Hg
* 11-Sb, As, Be, Cd, Cr, Pb, Mn, Ni. Se, Co,& Hg
* 11-Sb. As, Be. Cd. Cr, Pb, Mn, Ni, Se. Co.S Hg
Date Time Received by:
Date Time Received for Lab by: k
-------
fiWi'fc •••••>>• • •
fei^*" -
•j Custody Seal i Absent Sample Seals i Abs
i ^^:l Clie
d^tr**'
Project Number 46705 I Book
nL: PES03 - Pacific Environmental Services |
I 218
Dote Received | 09/15/98 | Dy^Z^f^^L^J^rT Page
Box HO COOLANT Temp 25.0 C Carrier and Number j MARSHALL CANNON | 12
•
1
1
till Number Client Sample ID Matrix
nR/HiCPM Client COC ID * Location
(218-12-1 - AC1B LIQUID AC
| ACID METALS LAB
|218-12-2 AC2B LIQUID AC
'| AC2B METALS LAB
|218-12-3 RAP2D/AC ASPII. CEMENT
| RAP2B/AC METAI.S LAB
7218-12-4 I! RAP2B/AOO AGGREGATE
J( RAP2B/AGO METALS LAD
|218-12-S . AC3B LIQUID AC
| ' AC3B METALS LAB
t
/
t
}
i.
218-12-C RAP3M2/AC ASPII. CEMENT
RAP3M2/AC METALS LAB
218-12-7 RAP3M2/AOO AGGREGATE
RAP3M2/ACX1 METALS LAB
218-12-8 AC4B LIQUID AC
AC4B METALS LAB
218-12-9 RAPSB/AC ASPII. CEMENT
« RAPSB/AC METALS LAB
218-12-10 -*Oai~ %flP5&ffl&& AGGREGATE
RAPSB/AGQ ___ * METALS LAB
|
1
To LAB
Date/Init
*
.
Receiving^ Remarks i SAMPLES RCC'D IN BOX - NO COOLANT
i! i'«
'(Archive Remarks i
TO STORAGE)
Date/Init
To LAB
Dat.e/Init
vised 05/27/1997 -- Page
TO STORAGE)
Date/Init
J
'
To I.AU
Date/Init
, .
1.
i'
TO STORAGE)
Date/Init
..
1
To LAB
D^te/Init
To STORAGE
Datc/Inlt
DISPOSED
D.iLo/Inlt
f
f
—
,
ro
-------
09/22/98
11:22
TRIANGLE LABORATORIES, INC.
Percent Moisture/Solid Calculations
Project: 46705-B
PRDPERC V4.01
Page: 1
>le Empty Wet Vial Dry Vial
:rd Vial.Wt Weight... Weight... Entered.By.
Date
Valid Weight Target
Time. . . . %Moist *Solid From -To Weight...
13.5299 15.6302 15.6256 WALTERS
13.5299 15.6302 15.6215 DURHAM
13.5299 15.6302 0.0000 JONESL
09/18/98 15:40:17
09/18/98 07:19:28
09/17/98 14:11:48
0.4 99.6
9.6386-10.4418
10.0402
13.5185 15.6937 15.6852 WALTERS
13.5185 15.6937 15.6843 DURHAM
13.5185 15.6937 0.0000 JONESL
09/18/98 15:40:18
09/18/98 07:19:28
09/17/98 14:11:48
0.4
99.6
9.6386-10.4418
10.O402
13.4318 15.7760 15.7649 WALTERS
13.4318 15.7760 15.7627 DURHAM
13.4318 15.7760 0.0000 JONESL
09/18/98 15:40:18
09/18/98 07:19:29
09/17/98 14:11:48
0.6
99.4
9.6579-10.4628
10.0604
rcent Moisture/Solid Summary
[.MILES.ID.... TLI.Number.
705-B -002 218-12-4
705-B -004 218-12-7
705-B -006 218-12-10
Client.Id.Number.
RAP2B/AGG
RAP3M2/AGG
RAP5B/AGG
%Moist %Solid ExtrctWt DryWtEqu RPD.
0.4 99.6
0.4 99.6
0.6 99.4
* End of Report ***
13
-------
PAGE 1 OF :.
IKJ^UHiUS UUJUKATUK1BS, INC,
Sample Preparation Tracking 4 Management Form
Project: 46705B Client: Pacific Environmental Services (PESOS)
Method: »JUOU H Extraction Data:
Solvent/Acids 0= M(V> -HCl' V^O Lot: IISOIO/^'
SamoLe Information
MJm7)An
1 / |1SU?1 ^L, «* i i i i i
| TLI / / | Sample ° | Final«HrH6 1 1 1 I |
Sample | SAMPLE ID / CLIENT '¥^)/ Vol 1 Volume 1 //I//I//I//I//I//
f crd | / SAMPLE ID | W / ml | ml | | | | | |
B | TxTilaHK | | 1 1 1 1 1 |
000 | TLI Blank | — | J(X) 1 1 1 I ' | |
B | 218-12-4 | |
002 | RAP2B/AGG \fy£)\ft '
B | 218-12-7 | |
004 | RAP3M2/AGG lQ.5101 '
B | 218-12-10 U«T/ll '
006 | RAP5B/AC3G iQOoi 1 1
B | 218-12-10DOP | |
007 | RAP5B/AGG |().0|3 1
B | 218-12-10 MS | |
008 | RAP5B/AGG l{).5l|p '
B | 218-12-10MSD | |
009 | RAPSB/AGG (^Oftf '
1 1 1 1 1 1
1 1 1 1 1 1
1 1 1 1 1 1
1 1 1 1 1 1
1 1 1 1 1 1
1 1 1 1 1 1
I 1 1 1 1 1
1 1 I 1 1 1
i 1 1 1 1 1
1 1 1 1 1 1
I 1 1 1 1 1
rl 1 1 1 1 I
B | LCS III 1 I I | |
010 | LAB CONTROL SPIKE | •""""" | \hh I I | | | |
1 1 1 1 1 1 1 1 1
1 1 1 1 1 1 1 1 1
1 1 1 1 1 i 1 1 1
1 1 1 1 1 1 1 1 1
1 1 1 1 1 1 1 1 1
1 1 1 1 1 1 1 I i
1 1 1 1 1 1 1 I 1
1 1 1 1 1 1 1 1 1
1 1 1 1 1 1 1 1 1
1 1 1 1 1 1 1 1 1
+--- + -
Comments •.
Iftnl. of
d
- —REV 07/26/93 (PSTMP 7)-
-------
PAGE
INORGANICS SPIKE LOG
DATE
- Ktfl
'
..
PROJECT *
SAMPLE IDs
i(0TQ56" ^-CS
3/8- 11- ID MS
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ORIGINAL
STANDARD
CONG.
(PPM)
X
>
•
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SAMPLE
RNAL
VOLUME
(mL)
O%M
SPIKE
SAMPLE
(PP8)
*
INITIALS
un
vl/A-ft, f
u/f
WITNESS
&U& '
J
8—*'
•
15
-------
* SEE SPIKE LOG
Project*
EXPdate
en/99
en/99
en/99
an/99
an/99
an/99
an/99
an/99
an/99
en/99
8/1/99
6/1M99
4/1/99
an/99
an/99
B/1/99
an/99
8/1/99
e/i/aa
an/99
en/99
an/99
an/99
8/1/99
an/ss
Spiking Standard Preparatfcm
itemont Standard Orig-Std. Spik»(uL)
ID
to
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|
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to
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354-7
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3*4-7
»64-7
3404
3404
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3404
3404
340-8
3-60-8
3404
340-SJ
344-7
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3*4-7
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3-eo-e
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3404
340-8
3404
340-7
(ppm) FvolpOOmL)
100
100
100
10000
100
100
100
100
10000
100
100
100
100
100
10000
1000
1 0030
100
10000
100
100
100
toco?
100
100
100
ICO
100
ICO
100
100
1000
5000
5000
gyr?
950
5000
5000
5000
5000
950
6000
5000
5000
soco
5000
950
£000
1500
SCCO
sso
soco
SCCO
sooo
7 SSO
sooo
SCCO
eoan
lj!^^p
f^f^f
SCCO
SCCO
soco
1500
cone
(ppm)
s
5
s
96
s
s
5
s
95
s
s
s
5
5
95
50 '
tsc
5
55
5
5
S
795
S
5
S
5
5
5
S
5
15
SPIKING
com Spiking Standard
lpike(uL) cone
FVol(100ml)
1000
1000
1000
1000
1000
1000
1000
1000
1000
1000
1000
1000
1000
10CO
1000
1000
toco
1000
toco
1000
TOCO
1000
TOCO
1000
toco
1000
1000
1000
1000
1000
1000
1000
(PPb)
so
so
so
950
so
so
so
50
950
so
so
so
50
50
950
SCO
(500
SO
sso
so
50
50
TS60 j
SO
50
50
SO
SO
so
so
50
150
combined
total
1000 1
1000
2003
toco
2COO
SCO
••Spika sopontaly
Etoment OrigStd
FvolflOOm
Au
Ca
Li
P
Pd
Pt
S
Si
Sn
Sr
1000
1000 -
1000
1000 •
1000
1000
1000
10000
1000
1000
140
30
70
100
160
300
360
SO
20
S
• 1400 '
300
- 700
-• 1000 -
1600
9000 -
3600 ''
SOOO
200
SO
10OOuL of ma Spiking Standard gives tha feted cone, of the above atamonto.
Spiking Standard 3-62-1
EXP: 10/28/98
Sp/Jrad
Predigeetion-
Pootdigaobon-
-------
PAGE 1 OF 1
TRIANGLE LABORATORIES, INC.
Transfer Chain-of-Custody Form
Project 46705-B
Transfer From:
Initials..
Released by:
Accepted by:
To: IA
Date
Time
n :
MILES.ID.
46705-B
46705-B
46705-B
46705-B
46705-B
46705-B
46705-B
46705-B
TLI NO,
Cust.Id.
-000
-002
-004
-006
-007
-008
-009
-010
TLI Blank
218-12-4
218-12-7
218-12-10
218-12-10DUP
218-12-10 MS
218-12-10MSD
LCS
TLI Blank
RAP2B/AGG
RAP3M2/AGG
RAP5B/AGG
RAP5B/AGG
RAP5B/AGG
RAP5B/AGG
LAB CONTROL SPIKE
Additional comments or instructions:
-XfrCOC (Rev 11/01/94)--+
-------
.-• ':i*W!
! VI tf?5
r'^Wii
k- ''-ffift
-------
SEE SPIKE LOG
EXPdate
8/1/99
an/ss
6/1/99
8/1/99
Wt/99
8/1/99
8/1/99
8/1/99
en/aa
8/1/99
8/1/99
671/93
8/1/39.
8/1/99
Bfl/SS
4/T/99
en /as
8/1/39
8/1,99
en/93
en/93
en/as
a/i/se
en/aa
8/1/99
en/99
an/99
en/99
en/99
en/99
| Spiking Standard Preparation
ftement Standard Orig. Std. Spika{uL)
1] ID (ppm)
r9
p
Kl
in1
B
jBa
r*
|Ca
pa
Cd
Co
br
Cu
I9
ra
k
k
Mg
tag
Mn
r°
Fa
r*
U
rb
Bb
3*4-7
3«xe
3*4-7
«&€
3-54-7
364-7
M08
36C-8
L 3*0-10
330-8
3*0-8
J60-8
3-c&«
3«>«
340-9
>S4-7
3-»5-5
3«>«
*5&5
3«&a
3«W
3«4-T
3^X3
>e&e
3-«CH?
3-eo-e
Be 1 MO*
r
F
V
pi
&
3«J-S
3«&e
3««
3-30*
MO-7
100
100
100
10000
100
100
100
100
10000
100
100
100
100
100
100CO
1000
10000
100
TOCOC
100
ICO
100
ICCOC1
100
1CC
1QC
100
100
100
100
100
1COO
FvolflOOmL)
5000
5000
5000
950
5000
£030
5000
5000
950
5000
5000
scoo
5000
5000
950
5CCO
TS33
5000
950
SOOO
5000
3XO
19SQ
5000
SCCO
sxx
SCCO
5000
5000
SCCO
5000
1SCO
cone
(ppm)
5
5
S
96
5
S
5
5
95
S
5
5
S
5
95
50
fSJ
5
45
S
5
5
:°S
5
5
5
5
S
S
S
5
15 __i
SPIKING
'rom Spilling Standard
3pike(uL) cone
=Vol{100irtL
1000
1000
1000
1000
1000
1000
1000
1000
1000
1000
1CCO
1000
1000
1CCO
1000
1000
toco
1000
1CCO
1000
1000
1000
1000
1COO
1CCO
1000
1000
10CO
1CCO
1000
1CCO
1CCO
(PPb)
50
50
50
960
50
50
so
so
950
so
50
50
50
50
950
SCO
tsoo
SO
*50
SO
50
SO
1950
50
50
SO
50
SO
so
so
so
150
combined
total
1000
1000
1000
2037
TOCO
2000
300
"Spika separately
Element Orig Std'
Spikeful) cone
FvolQCOm (ppo)
Au
C*
U
P
Pd
Pt
S
SI
Sn
Sf
1000
1000
1000
1000
1000
1000
1000
10000
1000
1000
140
X
70
100
180
300
360
50
20
5
1400
300
700
1000
1600
3000
3500
SCCO
200
SO
1 COCuL of tha Spiking Standard giveo t^e listed cone, of tne above elements.
Spjking Standard 3-62-2
EXP: 10/28/98
Sp/*ocf by:
19
-------
PAGE 1 OF 1
Project: 46705
Method:
1 Solvent/Acids 0:
TRIANGLE LABORATORIES, INC.
Sample Preparation Tracking & Management Form
Client: Pacific Environmental Services (PES03)
ample Information
Extraction Date
Lot:
.Sample Infgfcma
" i^r^ I O
! I
! | TLI /
| Sample | SAMPLE ID / CLIENT
I* crd| / SAMPLE ID
wff
A
|gt/ Vol (Volume] / / |__/J,/- 1 /
|(g//ml | ml
|B | TLI Blank
!°°°
1
MR P)
TLI Blank
..^
1 /O C'
\
\
,B | 218-12-4
|002 |
1
RAP2B/AGG \
\\J .
|B | 218-12-7
1004 |
RAP3M2/AGG
i0.(?7l
|B I 218-12-10
006 I
L 1 1
RAP5B/AGG (,,>.
lO
|B | 218-12-10DUP
|007 |
RAP5B/AGG
o,:
o.wi
(Wit. !o-M
IB
|009
IB | LCS
1 010
I
LAB CONTROL SPIKE |
Jf
7aJ/'T'.£ijo_i
.r..ru>.
10,75^
I Comments :C\DQ
3a
-\, Sti
.ga&KWrrmr •*&!»*
'ihUBW. uyiS U£ec!> -V
07/26/93 (PSTMF 7)--t
Pf
-------
PAGE
MERCURY SPIKE LOG
DATE
PROJECT #
SAMPLE IDs
ORIGINAL
SPIKE
CONC. (Hg)
STANDARD #
WORKING
STANDARD
PREPARED
FROM
SPIKE
AMOUNT
(mg
SPIKE
SAMPLE
(PPB)
INITIALS WITNESS
-3-W-fl
5
SL
-
]r
H1.5)S.t@>
fl-
ipflm
. 5
4i4a
0.
3-M-6.
5
\/
i
. ,
'3
5 -/£
? /r.
5
5
\r
I
«-!»*•*«
4(p5046 f^T)
•f
i
201
aa\forms\hgspke.tog (08/22/96)
21
-------
PAGE
MERCURY SPIKE LOG
DATE
PROJECT *
SAMPLE IDs
ORIGINAL
SPIKE
CONG. (Hg)
STANDARD #
WORKING
STANDARD
PREPARED
FROM
SPIKE
AMOUNT
(mL)
SPIKE
SAMPLE
(PPS)
INITIALS
-A.
WrTNESS
5'
cf-
i
qa\forms\hgspke.log (08/22/96)
22
-------
SAMPLE
DATA
aoTCapapfcOrfrt Rgg«t»BMr
819*44*723 F*X * 919*44*491
23
-------
Client: Pacific Environmental Services
Project Number: 46705B
Sample Report
Client Sample ID:
TLI Sample ID:
Date Received:
Date Prepared:
Date Analyzed:
Matrix:
RAP2B/AGG
218-12-4
September 15. 1998
September 16, 1998
September 20-21. 1998
Aggregate
.#&? ^rsH
'- Analvte. '4K
As
Be
Cd
Co
Cr
Mn
Ni
Pb
Sb
Se
v-.Cqnc,;^-
->/«&
24.702
1.100
3.220
33.331
67.106
1352.786
45.310
106.235
0.767
10.282
;, S^erceni s.<
99.6
99.6
99.6
99.6
99.6
99.6
99.6
99.6
99.6
99.6
^ytgranfey?*
-^IIUs^H^f
0.518
0.518
0.518
0.518
0.518
0.518
0.518
0.518
0.518
0.518
'~$*Ug£
•^RrattofS
100
100
100
100
100
100
100
100
100
100
~ .Dilution £
kltiicbril*
1
1
1
1
1
1
1
1
1
1
t mg/Kg
; Result ':-.
4.79
< 0.969
0.624
6.46
13.0
262
8.78
20.6
< 0.775
1.99
_
Triangle Laboratories, Inc.
801 Capitola Drive * Durham, North Carolina 27713
Tele: (919) 544-5729 * Fax: (919) 544-5491
Printed: 08-Sep-98 at 01:45PM
210
24
-------
Client: Pacific Environmental Services
Project Number: 46705B
Sample Report
Client Samcle ID:
TLI Sample ID-
Date Received:
Date Prepared:
Date Analvzed:
Matrix:
RAP3M2/AGG
218-12-7
September 15. 1998
September 16, 1998
September 20-21. 1998
Aggregate
, J4fcj ;%7,~^>^
•<-;^*>»'< J *£,.•&,*,
' Analvte - r
As
Be
Cd
Co
Cr
Mn
Ni
Pb
Sb
Se
tf^rt^l
">(ud/ui*i{
20.869
1.100
3.431
28.585
51.099
1237.938
45.859
113.184
-1.243
12.937
A&, .? «^**W«* '-* •ei.^t.^yt
•flRercera>
s ^^£Vj^**#«».**t'\!S'
'^•SoBeT*.'
99.6
99.6
99.6
99.6
99.6
99.6
99.6
99.6
99.6
99.6
p,^^#sH^,Si**fiWSS% •*-.
m^us&m*
0.512
0.512
0.512
0.512
0.512
0.512
0.512
0.512
0.512
0.512
>"-*& -^f^. „ "- .V-l'1^
'£ Rrial Vo\. .••*'
100
100
100
100
100
100
100
100
100
100
j;:j|dtQfi^j
^viFartDF^i
1
1
1
1
1
1
1
1
1
1
~£»K9^'
>^.:Result ii:,--;
4.09
< 0.98
0.673
5.61
10.0
243
8.99
22.2
< 0.784
2.54
Triangle Laboratories, Inc.
801 Capitola Drive * Durham, North Carolina 27713
Tele: (919) 544-5729 * Fax: (919) 544-5491
Printed: 08-Sep-98 at 01:45PM
-------
Client: Pacific Environmental Services
Project Number: 46705B
Sample Report
Client Sample ID:
TLI Sample ID:
Date Received:
Date Prepared:
Date Analyzed:
Matrix:
RAP5B/AGG
218-12-10
September 15. 1998
September 16. 1998
September 20-21. 1998
Aggregate
Analvte •„•:
As
Be
Cd
Co
Cr
Mn
Ni
Pb
Sb
Se
.Cone.™
(uo/tf %'--
33.548
1.100
3.400
36.858
64.161
1273.526
40.507
167.679
-0.516
11.478
, ^.Percent
- .,'-,^r*iKil!.''i-U.
Solid ~ "-
99.4
99.4
99.4
99.4
99.4
99.4
99.4
99.4
99.4
99.4
I warns >>
^'^lUset'f1
0.521
0.521
0.521
0.521
0.521
0.521
0.521
0.521
0.521
0.521
• :^.rriL'-'C\
RnaJWiX
100
100
100
100
100
100
100
100
100
100
Dilution s
•••? Factor" £
1
1
1
1
1
1
1
1
1
1
: rrig/Kg* •'...
""Result
6.48
< 0.965
0.657
7.12
12.4
246
7.82
32.4
< 0.772
2.22
Triangle Laboratories, Inc.
801 Capitola Drive * Durham, North Carolina 27713
Tele: (919) 544-5729 * Fax: (919) 544-5491
Printed: 08-Sep-98 at 01:45PM
-------
Client: Pacific Environmental Services
Project Number; 46705B
Sample Report
Client Sample ID:
TLI Sample ID:
Date Received:
Date Prepared:
Date Analyzed:
Matrix:
RAP5B/AGG
218-12-10 L
September 15. 1998
September 16, 1998
September 20-21. 1998
Aggregate
Anafvte -
As
Be
Cd
Co
Cr
Mn
Ni
Pb
Sb
Se
„ Conc.r-?^
(ug/L);x
6.616
N/A
0.844
7.552
13.714
262.057
8.552
33.681
0.427
2.110
:f£ercenf,,^
99.4
99.4
99.4
99.4
99.4
99.4
99.4
99.4
99.4
99.4
0.521
0.521
0.521
0.521
0.521
0.521
0.521
0.521
0.521
0.521
100
100
100
100
100
100
100
100
100
100
'-., -#•' —*'.,*&&**&* .,»««<
; .
-------
Client: Pacific Environmental Services
Project Number; 46705B
Sample Report
Client Sample ID:
TLI Sample ID:
Date Received:
Date Prepared:
Date Analvzed:
Matrix:
RAP5B/AGG
218-12-10 D
September 15. 1998
September 16. 1998
September 20-21. 1998
Aggregate
'^ > Aneuvte $8
As
Be
Cd
Co
Cr
Mn
Ni
Pb
Sb
Se
^fcCono^
*&ffl5&
28.651
1.000
3.418
39.240
101.407
1211.558
51.413
165.564
0.701
11.620
^Percent,*,
<-!-ifeij*"~* *** '>-*"£•'•• fJi -~
vf^sofid^
99.4
99.4
99.4
99.4
99.4
99.4
99.4
99.4
99.4
99.4
0.513
0.513
0.513
0.513
0.513
0.513
0.513
0.513
0.513
0.513
-?Rrfefer5
100
100
100
100
100
100
100
100
100
100
DilutioivS
• rFacJorf S
1
1
1
1
1
1
1
1
1
1
.
..,.:yjng/Kfl %, '[
'•*:itesyt '•-
5.62
< 0.981
0.670
7.70
19.9
238
10.1
32.5
< 0.784
2.28
.
Triangle Laboratories, Inc.
801 Capitola Drive * Durham, North Carolina 27713
Tele: (919) 544-5729 * Fax: (919) 544-5491
Printed: 08-Sep-98 at 01:45PM
28
-------
Client: Pacific Environmental Services
Project Number: 46705B
Sample Report
Client Sample ID:
TLI Samole ID:
Date Received:
Date Prepared:
Date Analyzed'
Matrix:
RAP5B/AGG
218-12-10 MS
September 15. 1998
September 16, 1998
September 20-21. 1998
Aggregate
" r^'-'vr4, ''**<,! ^"i,\;'f^
"'-'• Analvte^
As
Be
Cd
Co
Cr
Mn
Ni
Pb
Sb
Se
-if^Cono-i^
'^'(\x^K
78.042
N/A
51.592
82.049
110.244
1295.977
89.290
221.732
16.527
55.014
^Percent's
99.4
99.4
99.4
99.4
99.4
99.4
99.4
99.4
99.4
99.4
0.516
0.516
0.516
0.516
0.516
0.516
0.516
0.516
0.516
0.516
r';FirIitdW
100
100
100
100
100
100
100
100
100
100
^piiMfionl-i
^"-Fae{orf-:
1
1
1
1
1
1
1
1
1
1
_*-£~ v V-*- u_ »
§^npKg .,- __•
* -Result
15.2
N/A
10.1
16.0
21.5
253
17.4
43.2
3.22
10.7
= _
Triangle Laboratories, Inc.
801 Capitola Drive * Durham, North Carolina 27713
Tele: (919) 544-5729 * Fax: (919) 544-5491
Printed: 08-Sep-98 at 01:45 PM
29
-------
Client: Pacific Environmental Services
Project Number; 46705B
Sample Report
Client Sample ID:
TLI Sample ID-
Date Received:
Date Prepared:
Date Analyzed:
Matrix:
RAP5B/AGG
218-12-10 MSD
September 15. 1998
September 16. 1998
September 20-21. 1998
Aggregate
•! Analvte >
As
Be
Cd
Co
Cr
Mn
Ni
Pb
Sb
Se
,: ,i;Cona %
••*•*•&&&%
85.967
N/A
49.275
81.726
109.101
1146.941
87.128
217.105
15.480
55.212
99.4
99.4
99.4
99.4
99.4
99.4
99.4
99.4
99.4
99.4
Slarafwi*
0.572
0.572
0.572
0.572
0.572
0.572
0.572
0.572
0.572
0.572
^SsjMT^
.-"^^yS-.-aer:'
: Final Vol.
100
100
100
100
100
100
100
100
100
100
Dilution :7
-'••ftSfr^
1
1
1
1
1
1
1
1
1
1
LS>«Mr:'--
TS-jtear^--
15.1
N/A
8.67
14.4
19.2
202
15.3
38.2
2.72
9.71
Triangle Laboratories, Inc.
801 Capitola Drive * Durham, North Carolina 27713
Tele: (919) 544-5729 * Fax: (919) 544-5491
Printed: 08-Sep-98 at"" 01:45 PM
30
-------
Client: Pacific Environmental Services
Project Number: 4670SB
QA: Serial Dilution
Client Sample ID:
TLI Sample ID-
Date Prepared:
Date Analyzed:
Matrix:
RAP5B/AGG
218-12-10
September 16. 1998
September 20-21. 1998
Aeereeate
RAP5B/AGG
218-12-10 L
September 16. 1998
September 20-21. 1998
Afierepate
Analyte
As
Be
Cd
Co
Cr
Mn
Ni
Pb
Sb
Se
Native Sample
---...' mg/Kg Ji
• Result -"--
6.48
< 0.965
0.657
7.12
12.4
246
7.82
32.4
< 0.772
2.22
-i^ugrti.'' ,>
Cone. ""
33.548
1.100
3.400
36.858
64.161
1273.526
40.507
167.679
-0.516
11.478
Serial Dilution
-•^-;BBsfflt.'#
6.39
N/A
< 0.965
7.29
13.2
253
8.26
32.5
< 3.86
< 2.90
u!is*gfcs&,
•> .-*v- '** -" ^ '-y--
'--',=-, Cone; -~<
6.616
N/A
0.844
7.552
13.714
262.057
8.552
33.681
0.427
2.110
—.
"' ~-i.-£~"~ ,
* '-' *'y'*tr ' ^ '
4fleD;i
M: •*-3ir "
v .Tis<"r5 'f
-------
Client: Pacific Environmental Services
Project Number: 46705B
QA: Duplicate
Client Sample ID:
TLI Sample ID:
Date Prepared:
Date Analyzed:
Matrix:
RAP5B/AGG
918-12-10
September 16. 1998
Sentemher 20-21. 1998
Aggregate
RAP5B/AGG
218-12-10 D
September 16. 1998
Sentember 20-21. 1998
Aggregate
; '*'';': ~H »'''.*« -V, ..,'
"Ahalvte " ?
As
Be
Cd
Co
Cr
Mn
Ni
Pb
Sb
Se
Sample
t'^.-^Resllr**
6.48
< 0.965
0.657
7.12
12.4
246
7.82
32.4
< 0.772
2.22
33.548
1.100
3.400
36.858
64.161
1273.526
40.507
167.679
-0.516
11.478
Duplicate
iPfefResffitli
5.62
< 0.981
0.67
7.70
19.9
238
10.1
32.5
< 0.784
2.28
7^g,ug/L>SM»
28.651
1.000
3.418
39.240
101.407
1211.558
51.413
165.564
0.701
11.620
l$6ij!p?£
'vfesfdt^^t^- v '•>
?^^?grj& --
-------
Client: Pacific Environmental Services
Project Number: 46705B
QA: Matrix Spikes (Pre-Digestion)
Client Sample ID:
TLI Sample ID:
Date Prepared:
Date Analyzed:
Matrix:
RAP5B/AGG MS
9.1 8-12-10 MS
September 16. 1998
September 20-21, 1998
Aeeregate
RAP5B/AGG MSD
218-12-10 MSD
September 16. 1998
September 20-21, 1998
Aggregate
•V.' "T: \ '""'
Analyte
As
Be
Cd
Co
Cr
Mn
Ni
Pb
Sb
Se
Matrix Spike
'•^Result^
mq/Ka : '''••
15.2
N/A
10.1
16.0
21.5
253
17.4
43.2
3.22
10.7
^True£pike,^f|
if «. -VH^fSjrigyjSait
-: mq/Kq -t'*
9.74
N/A
9.79
9.75
9.75
9.76
9.74
9.74
9.74
9.72
Recovery
90°/c
N/A
967<
91 7<
937<
Spike Low
987<
111°/<
257<
87°/<
Matrix Spike Duplicate
.; " mq/Kg"r
15.1
N/A
8.67
14.4
19.2
202
15.3
38.2
2.72
9.71
TrueSpi^
mg/Ka
8.78
N/A
8.80
8.81
8.80
8.81
8.78
8.80
8.79
8.79
—
'•,«*-...•;
Recovery
987<
N/A
91 7<
837.
77°/<
Spike Low
857c
667c
227<
857<
RPD
,„ 'jf, '-^"
0.660%
N/A
15.2%
10.5%
11.3%
22.4%
12.8%
12.3%
16.8%
9.70%
—
—
—
—
— .
—
—
—
—
—
—
—
—
—
—
—
—
—
—
_-
—
Triangle Laboratories, Inc.
801 Capitola Drive * Durham, NC 27713
Tele: (919) 544-5729 * Fax: (919) 544-5491
Printed: 08-Sep-98
at
01:46PM
33
-------
Client: Pacific Environmental Services
Project Number: 46705B
QA: Matrix Spikes (Post-Digestion)
Client Sample ID:
TLI Samcle ID:
Date Prepared:
Date Analyzed:
Matrix:
RAP5B/AGG PDS
218-12-10 PDS
September 16, 1998
Seotember 20-21. 1998
Aggregate
Analvte
As
Be
Cd
Co
Cr
Mn
Ni
Pb
Sb
Se
Post-Dig
Recovered >
Amount (uq/L)
79.82
N/A
51.44
86.58
113.01
1X9.49
89.72
216.00
47.78
56.69
stion Spike
•f'Anridjirfro^S^
50
50
50
50
50
50
50
50
50
50
Recovery
93°/c
N/A
96°/<
99°/<
98°/<
Soike Low
98°/«
97°/«
967<
90°/<
Post-Digestion Spike Duplicate
^Becx)vere<• r# ^'^^^f^^C&jg ^ vi
'Amount (uoO^^
-
. .
f *< '% -W
V,?'. .-"» >i-;-.
•:Recoven/
-
"£ *X,<^^t*Sj§WS^£,J
•^RPdj\
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Triangle Laboratories, Inc.
801 Capitola Drive * Durham, NC 27713
Tele: (919) 544-5729 * Fax: (919) 544-5491
Printed: 08-Sep-98
at 01:46PM
-------
Client: Pacific Environmental Services
Project Number; 46705B
QA: Method Blank
TLI Sample ID:
Date Prepared'
Date Analvzed:
Matrix:
46705B MB
September 16. 1998
September 20-21. 1998
N/A
. ,X*£^, ' -\^f s
'. '"Analvte-
As
Be
Cd
Co
Cr
Mn
Ni
Pb
Sb
Se
Method Blank
;,vRef»yered;.:4!
^Amoffhtfuot.)
-2.68
0.0
-0.08
-0.55
-0.22
0.49
-2.71
0.48
0.18
-0.62
^>Brrn^5flL>"S "*••-' ^'3x '-., '
5
5
1
2
2
2
3
2
4
3
—
—
—
—
—
—
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—
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—
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—
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Pass
Pass
Pass
Pass
Pass
Pass
Pass
Pass
Pass
—
—
—
—
—
—
—
—
—
...
—
—
—
—
—
—
—
—
„
—
—
Triangle Laboratories, Inc.
801 Capitola Drive * Durham, NC 27713
Tele: (919) 544-5729 * Fax: (919) 544-5491
Printed: 08-Sep-98
at
01:46 PM
•zz
-------
Client: Pacific Environmental Services
Project Number: 46705B
QA: Lab Control Spikes
TLI Sample ID:
Date Prepared:
Date Analyzed:
Matrix:
46705B LCS
September 16, 1998
September 20-21, 1998
N/A
Anafyte
As
Be
Cd
Co
Cr
Mn
Ni
Pb
Sb
Se
Lab Control Spike
: .Recovered./?;
AmotmWuo/LJ'
44.49
51.00
49.79
50.46
51.15
51.36
47.46
50.90
49.21
45.15
' - ^XmoSn^^Sf •;•
50
50
50
50
50
50
50
50
50
50
' "'•^S^^j^*^^
:Recwen£'
89°/<
102%
100%
1010/
102°/<
103°^
95°/<
102°/c
98°/c
90°/
Lab Control S
; . -. Recovered*^ .£&?-«•
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pike Duplicate
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__
__
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—
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— .
—
—
Triangle Laboratories, Inc.
801 Capitola Drive * Durham, NC 27713
Tele: (919) 544-5729 * Fax: (919) 544-5491
Printed: 08-Sep-98
at 01:46PM
36
-------
Client:
Project Number:
Pacific Environmental Services
46705B
Sample Report
Date Received:
Date Prepared:
Date Analyzed:
DATA FILE:
Matrix:
Seotember 15, 1998
SeDtember21.1998
September 22. 1998
AB
Aeereeate
ANALYTE: Ha
uo/LRDL 0.2
Analysis Method:
7471
Instrument P E Zeeman 5100
Soike Cone. (uo/U
5
CVAA ANALYTE SUMMARY REPORT
RAP2B/AGG
RAP2B/AGG D
RAP3M2/AGG
RAP3M2/AGG D
RAP5B/AGG
RAP5B/AGG D
RAP2B/AGG MS
RAP2B/AGG MSD
RAP2B/AGG MS
RAP2B/AGG MSD
Method Blank
Method Blank D
LCS
LCSD
TLI SAMPID
218-12-4
21 8-1 2-4 D
218-12-7
21 8-1 2-7 D
218-12-10
21 8-1 2-1 OD
21 8-1 2-4 MS
21 8-1 2-4 MSD
True Spike MS
True Spike MSD
46705B MB
46705B MBD
46705B LCS
46705B LCSD
ug/L
CONG
0.114
0.010
0.253
0.302
0.266
0.315
4.286
4.271
5
5
0.039
0.021
4.596
4.962
ml
MPV
100
100
100
100
100
100
100
100
100
100
_
—
-
gram wt
USED
0.742
0.814
0.674
0.754
0.768
0.828
0.634
0.661
0.634
0.661
_
—
-
Percent
Solid
99.6%
99.6%
99.6%
99.6%
99.4%
99.4%
99.6%
99.6%
99.6%
99.6%
_
—
__
OIL
FACTOR
1
1
1
1
1
1
1
1
1
1
_
—
-
RESULT
< 0.027
< 0.025
0.038
0.040
0.035
0.038
0.679
0.649
0.792
0.759
_
—
__
Avg.
RESULT
< 0.026
•ff 0.039
•f. 0.037
_
—
_
—
— "..-"'^
RPD
-
-
-
4.52%
—
_
—
..__...
%REC
—
—
—
86%
85%
--
—
-92%-
99%
Triangle Laboratories, Inc.
801 Caprtola Drive * Durham, North Carolina 27713
Tele: (919) 544-5729 * Fax: (919) 544-5491
Printed: 23-Sep-98 at 11:10 AM
37
-------
"^.-•y *" *c -- f f
AutoSawler Reoorf Table: HA600
09-20-98 01:17:17 PH page 1
Table Naae: HA600 Autosaapler Type: TYPE TJA
Sample Positions: 179/192 JJC Position?: 13/19 I Sets: 2
Rinse Station location is rack -1, pos. -1.
1 Aux. (L) Rack STD/QC/BI
2 Sample (16mm) Saaples
3 Saaple (16«a) Saiples
4 Saaple (I6an) Saaples
5 Saiole (16m) Saaples
— Sasple Sets —
SetS Type Prepare? Description
1 Norsal No 465748
2 Normal No 467058'
--- Preoaration Info —
Sets Uotake I)otakc82 Final
No Saapies Prepared.
Rack
-------
» _ - . i . > t - —^--•-v_
:.-->•, -^rr .. - 37-, -~^-;--v- =..- ;•-
AutoSaipler Report Table: HA600
Rack 13
Pos ROH Col Sample Naie
(1...48 Not Used)
Rack 84
Pos ROH Col Sample Naae
(1...48 Not Used)
Rack OS
Pos ROM Col Sample Name
(1...48 Not Used)
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• Sun 09-20-98 01:17:17 PHrr^pag?'2--S^'M*.----"-^!!.-.
Set t tUsed Type
Set t tUsed Type
Set I tUsed Type
-------
•Analysis Report -
t Saiple Naie
Suaiary""
Sun 09-20-98.01:15313 PH page 1
File Method,. Date Tiie OpID Type Node
1
2
3
4
5
6
7
8
9
10
11
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13
14
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16
17
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465748 MB
46574B LCS
216-79-8,14
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46705'a M8
4670581CS
218-12-4
213-12-7
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/ iV 70
92098
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09/20/93
09/29/98
09/20/98
09/20/98
09/20/98
09/20/98
09/20/98
09/20/98
09/20/98
09/20/98
09/20/98
09/20/98
09/20/98
09/20/98
09/20/98
09/20/93
09/20/98
09/JO/98
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-------
Analysis Reoort Averages
Sun 09-20-98 01:09:17 PH -"page 9
^gs^i^r~^^sgp^
f s.-,.-*».^it»i«,—"• ... „_ _«*. v ^->.._—,.ki ,. jsi, >w.—,..,n gsa
Hethod: TRIAN6L2 Sauple Na«e: ICV/CCV v :. Operator: DHL „.-_._
Run Tiie: 09/25/98 11:09 " Filenaie: 92098
Hade: CONC Type: 0 Corr. Factor: 1.08000
Lab 10.: Cust". Sapl. 10.: Cust. ID.: 465748
Elans
Units
Avge
SDev
iRSD
Slams
Units
Avge
SOev
WSD
Eleus
Units
Avge
SOev
;RSD
Elems
Units
Avge
SOev
«SD
[le,io
Units
Avge
SOev
«50
•li-JIS
1111 i ^ J
A '.ye
SOev
WSG
ftg3280
ppb
501.4
2.J72
.4332
Ca3179
ppb
509.4
3.975
.7804
Fe2714
ODD
509. i
11. ol
2.279
Na3302
ppm
4.902
.0461
.9398
1960-1
ppb
511.8
.9554
.1363
7i33-i:;
DCO
505.5
2.26
.447
A13082
ppb
480.3
3.827
.7963
Cd2265
ppb
503.1
3.553
.7003
K.7664
ppm
5.033
.0572
1.136
N12316
ppo
504.2
3.357
.6653
1960-2
ppb
510.1
1.53
.299"
Tii^OS
000
506.9
4.352
.9572
AS1390
ppb
508.5
3.002
.5905
Ce4186
ppb
504.2
2.054
.4075
Li6707
PPO
491.9
7.714
1.563
P.2149
ODD
493.2
1.142
.2292
Pb2203
ppb
504.4
3.215
.6375
V_2924
OpO
504.3
2.839
.5o25
BJ496
opb
491.7
1.689
.3435
Co2286
ppb
511.3
3.452
.6752
Hg279Q
•ppb
501.3
3.955
.7832
2203-1
ppb
507.2
1.93
.3805
Sel960
H« V.
pyu
510.7
1.043
.2042
[n20o.
PPO
512.5
5.767
1.125
Ba4934
ppb
515.5
2.73
.5297
Cr2677
ppb
509.6
4.723
.9263
Mn2576
ppb
J510.7
3.016
.5907
2203-2
pQb
503.0
4.115
.3132
Snl899
Dpb
512.1
3.525
.6334
5123S1
oob
5007.
23. i
.4675
Be3130
ppb
504.8
3.33
.6597
Cu3247
PPb
508.1
2.639
.5193
M02020
ODD
510.3
n / - /
L . 000
.5162
5b2C63
poo
437.0
7.473
1.535
Sr4215
ODD
508.7
2.436
.4336
-------
iVlysiirReporlf:;>~">r."Averages"
Vun 09-20-98 .of:09:lf PN^"
ithod: TRIAN6L2 Sanple Naie: IC8/CCB w • Operator: OXH
in Tiae: 09/20/98 11:18 - Filenane: 92098
Jde: CONC Type: 3 Corr. Factor: 1.00000 —
ib ID.: Custr. Siol. ID.: Cust. ID.: 46574B
less
lits
/ge
)ev
^SD
leas
lits
/ge
Dev
USD
lens
nits
i/ge
Dev
RSO
leiBS
nils
vge
Dev
RSO
iaias
nits
vge
Oev
,RSO
lens
in.;s
iVyc
iDeV
,R£D
Ag32SO
ppb
-.2385
.974
408.4
Ca3179
ppb
.5744
1.113
194.6
Fe27U
9DD
5. 848
12.76
213.3
Na33C2
Jum
-.1742
.1916
110
1960-1
ppb
-.5542
.4766
85. 98
Ti5349
DpO
.1725
.1885
109. 3
A13082
ppb
-22.53
2.756
12.23
Cd2265
ppb
.2456
.2414
98.3
K.7664
PPi
.0240
.0339
141
Ni2316
opb
-.0526
.2319
441
1960-2
ppb
.1561
.6414
411
Tii'QS
DpO
o ^:n
i.-.'i
.3665
16.27
AS1890
ppb
.0613
.2133
347.7
C34186
ppb
1.260
3.709
294.5
Li6707
ppb
.1458
.0352
24.12
P_2149
OCu
.1157
5.769
4984
Pb2203
ppb
-.9504
.9324
93.11
V_2924
DOD
.2472
.484
195.3
B.2496
ppb
-16.44
1.238
7.533
C02286
ppb
.3539
.84
237.4
!ig2790
Ppb
.0441
a. 483
14700
2203-i
ppD
-3.715
1.457
39.23
S51960
poo
-.0305
1 1 / n
. OOOi
417.8
Zn2062
DOO
.3631
.564
155.3
8a4934
ppb
.1139
.0824
72.36
Cr2677
ppb
.4401
.8711
197.9
«n2576
pDb
j.0851
.0604
70.91
2203-2
pDb
.4299
1.466
341
SnlS99
ppb
-.6453
.2999
46.43
3; nn /^ i
lioal
Ouu
-112.8
6.276
5.565
Be3130
ppb
.0092
.0133
144.1
Cu3247
ppb
.7999
.4722
59.04
1102020
ODD
.3948
.3039
78.23
5b2063
OOb
.4329
1.179
244.1
Sr4215
PPb
.1060
.0276
26.05
-
-------
^""Analysis Report .- Averages
Sun 09-20-98 01:09:17'PH -'page'if
Operator: OKH
Method: TRIANGL2 Saople Naie: ICSAB v
Run Tine: 09/20/98 11:23 - Filename: 92098
Mode: CQNC Type: Q Corr. Factor: 1.00000
Lab ID.: Cuslr. Sad. ID.: Cust. ID.: 465748
Eless
Units
Avge
SOev
*RSD
El ens
Units
Avgs
SDev
*RSD
Eleais
Units
Avge
SDev
WSD
Eleas
Units
Avge
SDav
iRSD
Ela«i3
Units
Avge
SDev
SRSD
••lass
u n i : 3
Avge
SOev
;RSO
Ag3280
pob
551.1
1.125
.2042
Ca3179
ppb
456700.
1355
.2967
,Fe2714
ppb
181600.
453.2
.2523
Na3302
PPffl
5.390
.0774
1.315
1960-i
ODD
559.5
2.774
.4957
113349
PCJ
509.2
.949
.1563
A13032
ppb
524500.
1147
.2187
Cd2265
ppb
489.6
1.524
.3112
X_7664
ppa
16.49
.0583
.3567
Hi23i6
ppb
465.5
1.253
.2702
1960-2
ODD
543.1
1 . 7oi
.3138
Til 503
C2D
520.0
7.941
1.527
A31890
ppb
525.3
2.42
.4608
Ce4186
ppb
514.2
.609
.1134
Li6707
ppb
652.1
1.961
.3CC8
P.2149
000
Q634.3
5.934
.9354
?b2203
ODD
503.4
.4993
.0993
V.292*
ODD
J9"'.J
1.30i
.2605
8.2496
ppb
534.4
1.788
.3346
Co2286
ppb
494.6
1.583
.3201
«g2790
ppb
535200.
1509
.282
2203 -i
pOO
512.1
2.93
.5721
5el960
000
543.6
1.34?
.2453
Zn20o2
ODD
•J59.0
1.62
.353
8a4934
ppb
542.5
.7799
.1437
Cr2677
ppb
493.6
1.903
.3855
Mn2576
Ppb
.,478.2
1.304
.272o
2205-2
PPb
499.1
2.203
.1413
Snl899
ODO
524.5
2.953
.563
Si2831
pOb
5441.
12.38
.2276
8a3130
PPb
491.1
1.208
.2461
CU3247
pob
569.7
1.15
.2018
H02020
Ppb
505.8
2.609
.5159
Sb206S
poo
519.2
6vn •*
. J70
1.231
5r4215
POD
533.5
.9446
.1771
-------
lalysfs Retifrt --""'-Averages ^ . "•.""/'Sun W-20-98'"oi:I3:2Q" PH -7"page 1
ithod: TRIAN6L2 Saaple Naie: 467058 MB_ .. . Operator: DKH
in Tine: 09/20/98 11:45 - Filename: 92098 -
ide: CONC Type: S Corr. Factor: - 1.00000
ib ID.:" Cust-. Snl. ID.: • Cust. ID.: 467053
leas •
lits
/ge
)av
?SD
.eas
lits
/ge
Jev
?SD
. Asl890
ppb
L-2.685
1.84
68.52
N12316
opb
L-Z.712
.3233
11.92
Be3130
pob
L-.0414
.0235
56.81
Pb2203
opb
L.4808
.6344
131.9
Cd2265
ppb
L-.0825
.1113
134.9
SD2068
oob
L.1774
1.045
589.1
Co2286
ppb
L-.5500
.1459
26.52
Sel960
pob
L-.6181
.4139
66.96
Cr2677
ppb
L-.2153
.0712
33.08
Hn2576
ppb
L.4867
.0255
5.237
-------
.
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-------
lalysis RepoVt Averages-"'
•;'I'Sun 09-20-98 01:13:20 PH ._ page~£":~E:
Operator: OXH
athod: TRIANGL2 Saaole Naue: 218-12-4,.
jn Tine: 09/20/98 11:54 - Filenass: 92098 .
ode: CQNC Type: S Corr. Factor: - 1.00000
ab ID.: Custr. Sinpl. ID.: Cust. ID.: 467058
lens
nits
vge
Oev
RSD
Asi890
ppb
24.70
1.716
6.947
8e3130
ppb
1-5.554
.0108
.1953
Cd2265
ppb
3.220
.1025
3.182
C02286
ppb
33.33
.6402
1.921
Cr2677
ppb
67.11
.8321
1.24
ppb
1353
1.578
.1167
.-^.. _-;....•£-.«•*•£
lens
nits
vgs
Dev
Ni2316 Pb2203
ppb ppb
45.31 106.2
.6245 l.iS
1.378 1.565
Sb2068 Sel960
ppb ppb
L.7672 10.28
.7364 .8907
95.99 8.662
-------
Analysis Report ' Averages*
Sun 09-20-98 "of: 13:20 P« ^_:page''4
Method: TRIAN6L2 Saipla Hane: 218-12-7fc Oosrator: DKH
Run Tiae: 09/20/98 11:58 " Filenaae: 92098
Node: CONC Tyoe: S Corr. Factor: 1.00000
Lab 10.: Cusr. Siol. 10.: Cust. 10.: 467058
Elet-s
Units
Avga
SDev
iRSD
AS1890
ppb
20.87
.7193
3.449
883130
Dpb
L-3.069
.0347
1.13
Cd2265
ppb
3.431
.0292
.8517
Co2286
ppb
28.58
.1445
.5054
Cr2677
ppb
51.10
.1288
.2521
Hn2576
ppb
1238.
9.61
.7763
Eleas
Units
Avge
SOav
N12316
ppb
45.86
1.026
2.237
Pb2203
ppb
113.2
1.405
1.241
Sb2063 Sel960
ppb ppb
L-1.243 12.94
i.526 .5889
122.7 4.552
-------
lalysis. Report • "^Averages
Sun 09-20-98 01:13:20 PH page 5
Operator: DKH
ithod: TRIANGL2 Sample Naae: 218-12-M
jn Tiie: 09/20/98 12:03 - Filenaie: 92098
ode: CONC Type: S Corr. Factor: 1.00000
ab 10.: Cust-. Snpl, ID.: Cust. ID.: 46705B
leus
nits
vge
Dev
RSD
AS1890
ppb
33.55
1.479
4.409
883130
ppb
L-6.381
.0204
.3196
Cd2265
ppb
3.400
.2031
5.975
Co2286
ppb
36.86
.3651
.9904
Cr2677
ppb
64.16
.1644
.2562
Hn2576
ppb
1274.
1.961
.154
leas
Inits
ivge
iDev
iRSD
N12316 Pb2203 Sb2068 Sel960
pob ppb pob ppb
40.51 '167.7 L-.5160 11.48
.9076 .3696 1.183 .7629
.2204
229.:
6.647
-------
Analysis Report Averager
Sun 09-20-98 01:15:20 P« -.--page 6'
Method: TRIANGL2 Saiple Naae: 218-12-1Q.D Operator: DKH
Run Tiae: 09/20/98 12:08 - Filenaie: 92098
Mode: CONC Type: S Corr. Factor: 1.00000
Lab ID.: Cusir. Sapl. 10.: Cust. ID.: 46705B
[less
Units
Avgs
SDev
•iRSO
Asl890
ppb
28.65
1.411
4.926
8e3130
ppb
L-S.684
.0046
.0809
Cd2265
ppb
3.418
.1694
4.954
Co2286
ppb
39.24
.5381
1.371
Cr2677
ppb
101.4
1.117
1.101
Hn2576
ppb
1212.
9.884
.8158
EleiDS
Units
Avga
SDev
%RSD
Ni231o
ppb
51.41
.5722
1.113
Pb2203
ppb
165.6
2.617
1.581
Sb2068
ppb
L.7008
2.71
386.7
Sel960
ppb
11.62
1.22
10.5
-------
Analysis' Report'" .Average?3
Sun 09-20-98 01:13:20 P« page 7
Operator: OKH
ilethod: TRIANGL2 Saaple Hase: 218-12-10 MS
Run Tine: 09/20/98 12:12 - Filename: 92098
Mode: CONC Type: S Corr. Factor: 1.00000
Lao ID.: eusir. Snpl. ID.: Cust. ID.: 467058
El ems
Units
Avge
SDev
IRSD
AS1890
PPb
78.04
.9675
1.24
Be3130
ppb
42.37
.0974
.2298
Cd2265
ppb
51.59
.116
.2248
C02286
ppb
82.05
.3057
.3726
Cr2677
ppb
110.2
.3505
.3179
Mn2576
pob
1296.
2.983
.2302
Elans
Units
Avge
SOev
Ni2316
ppb
89.29
1.135
1.271
Pb2203 Sb2068
ppb ppb
221.7 16.53
1.361 .5989
.6136 3.624
Sel960
ppb
55.01
1.389
2.525
-------
Analysis Report Averages
Sun 09-20-98 01:13:20 PH page 8
Operator: DKH
Hethod: TRIANGL2 Saaole Naae: 218-12-1Q.HSD
Run Tiie: 09/20/98 12:17 ~ Filanane: 92098
Hode: CONC Type: S Corr. Factor: 1.00000
Lab ID.: CusiT. Siol. ID.: Cusc. ID.: 467058
clems
Units
Avge
SDev
USD
Asi890
ppb
85.97
.5274
.6135
3e3130
ppb
38.73
.0436
.1124
Cd2265
ppb
49.28
.1345
.273
Co2236
ppb
81.73
.1206
.1476
Cr2677
Ppb
109.1
.1631
.1495
Hfi2576
ppb
1147.
1.5
.1308
Eleas
Units
Avge
SDev
SRSD
Ni2316
ppb
87.13
.9933
1.14
Pb2203
ppb
217.1
.5385
.248
Sb2068
ppb
15.48
.5629
3.636
Sel960
ppb
55.21
1.69
3.062
-------
alysis" Report Averages-
09-20-98 01:13:20 ?K "page 9
Operator: DKH
Jthod: TRIANGL2 Saaole Naie: 218-12-10 PDS
in Tiae: 09/20/98 12:22 - Filename: 92098
jda: CONC Type: S Corr. Factor: 1.00000
ib ID.: Cusb. Sapl. ID.: Cust. ID.: 467058
leas
nits
vga
Dev
RSO
leas
inits
•vgs
)0ev
,R5D
AS1890
pob
79.32
.7798
.9769
N12316
DOb
89.72
.3259
.9206
SeoiiO
PPb
41.31
.3126
.7568
Pb2203
ppb
216.0
1.337
.8503
Cd2265
ppb
51.44
.539
1.048
Sb2068
ppb
47.78
1.497
3.134
Co228o
ppb
86.58
.5552
.6412
Sel960
opb
56.69
1.217
2.147
Cr2677
ppb
113.0
.1965
.1739
Mn2576
ppb
1309.
8.562
.6539
-------
Analysis Report Averages Sun 09-20-98 01:13:20 PM page 10
Method: TRIANGL2 Sample Nane: 218-12-10^1 Operator: DKH
Run Tiae: 09/20/98 12:26 - Filename: 92098
Mode: CONC Type: S Corr. Factor: 1.00000
Lab ID.: Cusfr. Sipl. ID.: Cust. 10.: 467053
Eleas Asl890 8e3130 Cd2265 Co2286 Cr2677 Mn2576
Units ppb ppb ppb ppb ppb ppb
Avge 6.616 L-1.146 L.8441 7.552 13.71 262.1
SOev .4493 .0104 .1333 .2423 .0907 .9263
SRSD 6.792 .9124 15.3 3.2C8 .6615 .3535
cless Niijio Pb2203 Sb2068 Ssi96fl
units pOb ppb ppb pOb
AvQc 3.352 33.63 L.4273 L2.110
OL'CV ,o\jjo .33uu *.. i > 6 i.^uo
i?S& ".435 2.465 509,5 61.03
-------
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no
-------
Analysis Report Averages
Sun 09-20-98 01:13:20 PH page 12
Operator: DKH
Method: TRIANGL2 Saaiple Nans: IC3/CC3 _
Run Tise: 09/20/93 12:41 - Filename: 92098
Mode: COHC Type: 3 Corr. Factor: 1.00000
Lab 10.: Cusir. Ssol. ID.: Cust. 10.: 467053
Eleiiis
Units
Avge
SOev
;RSD
clems
Units
Avge
SDav
SRSD
Eicins
Units
Avge
SDav
",RSD
ClciliS
ijfiltS
Avge
SDsv
*.RSD
El«5ii
Units
Avye
50ev
',RSD
IlcSi /
Avys /
iuav 1
iSiiO V
Ag3Z80
POP
.0882
.1035
117.4
Ca5179
pob
1.S53
.7785
42
re27l4
ppb
14.34
l.Srd
ij. iO
Na3302
DDi
-.1459
.1165
80.03
1960-1 ,
DOO /
-i/::
.y\i
ft.it
' 7133^
Cvu
.5oZO
.0915
.16.2?
A13082
ppb
36.41
2.778
7.631
Cd2265
ppb
.3498
.1049
29.98
K_7b64
ppu
-.0256
.0015
5.939
Ni231o
Dpb
.0932/
.246/
25/2
'1960-2
?Db
.3494
.3175
90.39
T \ ' i j '" ~
1 i ^ 7 \j (3
ppo
36.544
.7931
12.11
Asl390
__Pfii_—
-.3899
.3042
78.02
Ce4l86
ppb
4.485
1.457
32.48
Li67Q7
ppD
.1573
.0133
S.449/
?/itf
/til
' 2.690
2.124
78.95
?b22C3
ops
-1.33S
.9113
49.5?
V 2^2-
Did
1.411
.loo
11.55
B.2496
— (jl!)U
-17.18
1.169
6.805
C02286
ppb
.4485
.061
13.6
Mg2790/
ppb /
6/75
/.U4
18.53
2203-1
PPP
-3.044
.6904
22.63
Sil96C
Ppb
-.3102
.5217
163.2
Zn2062
3DO
. j /' 6 u
.4156
Ja493J__
ppb
.2415
.0401
16.61
Cr2677
PPb
.5167/
.my
74/6
'I1n2576
ppo
j.2455
.001
.4162
2203-2
PPb
-1.235
1.539
128.6
Sr.1859
POP
.2279
.2Co3
90.54
5i2381
C'UU
-203.0
4.097
—•—•—•?—•
tjB^^n
ppb
.3941
.0229
5.811 /
U2247
/Ob
-.5675
.1151
20.27
Ho2020
ppb
1.250
1.001
80.1
Sb2063
PPb
34.042
3.303
31.32
3r4215
DDu
.1986
.0083
4. -12
I^BWW^^^^
-------
Analysis Report Averages
Sun 09-20-93 01:13:20 PM page 13
Method: IRIANGL2 Sample Naue: IC8/CC8 v Ooerator: DM
Run Tiae: 09/20/93 12:47 - Filename: 92098
Mode: CONC Type: 3 Corr. Factor: l.OQOOO
Lab ID.: Custr. Siipl. ID.: Cust. 10.: 467055
Units
Avge
SDsv
MSO
Elais
Units
Avge
SDev
SRSD
cless
Units
Avge
SCev
MSO
EiaiJS
Uniu
Avga
SDev
WSO
" *: L -
•J11 i 15
Avge
SOev
Ago230
DDD
.1229
.3266.
265.3
vys
30s v
-------
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fti.it osampl
Element
-" ;_c
-------
'1'ement File: BE. GEL
1ement : Bs
'rint Data: Main-<-Suppl.
'rint: Calib. Curve
Analyst: HOLSTE
Peak Storage: 1 Repl./Sample
.'NSTRUME1MT: 4100 ZL
Javelength: £34.9 Peak
signal Tvoe: Zeeman Aft
lead Time: 3.0
Sample Replicates: £
standard Replicates: 5.
Technique: HGA Version: 7.30
SI it: 0.70 Low
Signal Measurement: Peak Area
Read Delay: 0.0 BOC Time: £
Spike Replicates: Same as Sample
:ALIBRATION:
Solutions ! ID
1
"* a 1 -i K R 1 .r, ri L' I C: T T"i »5 1 Q Kl I/
standard 1 ISTD1= £.5ug/L
Standard £ ! BTD£= 5.0ug/L
Standard 3 ISTD3= 10ug/L !
£0.0 and Concentration > 0. £ then Retry 1 times
Check #RSD on: Samples + Standards + Spikes + QC Samples
Recovery Measurements:
5 uL of 10 ug/L Standard at Location £ Gives 5.0 ug/L
Measure Recovery on Samples: 11,15
Add to QC Samples: Yes •/. Recovery Limits: 85 to 115
63
-------
QC:
#1 fl/S I QC Sample I Cone. Limits I AfterI Periodic I At ICount As
I i_OCw | ID ! Lower Upper ICalibl Check lEndl Sample
1 A ICV=3.0ug/L £.7 3.3
2 13 ICB -1.0 1.0
3 5 CCy=fe.®ug/L 4.8 7. £ X XX
4 8 CCB -1.0 1.® X X X
Run Periodic QC Samples: Every 10
Out of Limit Action: Reslope and Rerun Samples
Matrix Check Calculations:
•/. Difference for Dupls: No Locations:
% Recovery for Spike: No Locations: Cone:
-------
lement File: BE.GEL
ate: 09/SO/98
ata File: EB33i.DAT
echniaue: HGA
tlement : Be
Time: 14:19
ID/UJt File: UNTITLED
Calib. Type: Linear
Wavelength: 23-4.
Slit: 0.70 L
Lamp Current: 30
Energy: 60
ID: STD BLANK
Sea. No.: 00001
A/S Pos. : 0
Date: 09/20/98
L disoenssd: 5 from 0, 5 from 40, 10 from 0
eplicate 1 Time: 14:S1
eak Area (A-s): 0.001 Peak Height (A): 0.004
ackground Pk Area (A-s): 0.005 Background Pk Height (A): 0.013
lank Corrected Pk Area (A-s): 0.001
oneentrat ion (uq/L ; : 0. 1
L dispensed: 5 from 0, 5 from 40, 10 from 0
.'eplicate £ (Peak Stored)
eak Area (A-s): -0.000
• ackground Pk Area (A-s): 0.005
'lank Corrected Pk Area (A-s): 0.000
ioncentrat i on (uc/L ): 0.0
Time: 14; 2,i
Peak Height •/.) : 80. 01
iuto-zero
ID: bTDI= 2.5uq/L Sec. No.:
disoensed: 10 from 0, 5 from 40, 5 from 1
A/3 Pos.: 1
Date: 09
ID: STD BLANK
Sea. No. : 0000C
fi/S Pos. : 0
Date: 09/20/98
_iL dispensed: 5 from 0. 5 from 40. 10 from 0
^eolicate 1 Time: 14:27
-'eak Area (A-s): -0.000 Peak Height (A): 0.003
Background Pk Area (A-s): 0.00fr Background Pk Height
-------
-r-ec c ea i-'K Hrea \H — 5 •> : W.Wc;/
Concentration (uq/L ): £.7
uL dispensed: 10 from 0. 5 from 40. 5 from 1
Reolicate 2. (Peak Stored)
Peak Area (A-s); 0.027
Background Pk ftrea (fl-s): 0. 04£
Blank Corrected Pk ftrea (A-s): 0.028
Concentration (ug/L ): 2.7
Mean Cone (ug/L .>
2.7
Standard number 1 applied. C2. 53
Correlation coefficient: 1.00000
Time: 14:34
Peak Height (A): 0.155
Background Pk Height (ft): 0.213
SD : 0.02
Slooe: 0.0110
RSDC/.): 0. 7b
Be
ID: STD£= 5. »up/L
/ A/ A* ^ A/ A^ A/ A.- A/ A* ^V 'V A/ A^ A^ A/ A* A* A* A/ A*
Sea. No.: 00005
A/S Pos. j 1
Date: 89/20/
uL disoenssd: 5 froni 0, 5 from 40, 10 from 1
Repl ic-at s 1 Time: 14:36
Peak Area (ft-s): 0.059 Peak Height (ft): 0. 333
Background Pk ftrea : 5.8
Mean Cone (ug/L ):
.6
Time: 14:39
Peak Heiqht (A): 0.403
Background Pk Heiqht (ft): 0. 4o
SD : 0.26
RSDC/i): 4.69
Standard number 2 aoDlied. C5. 03
Correlation coefficient: 0.99112
Slooe: 0.0120
Be
ID: STD3= Itfug./L
Sea. No.: 00006
fl/S Pas.: 2
Date: 09/S0/
uL dispensed- 5 from i?i. 5 from 40, 10 from 2
r^ •- • i c- a t e 1 T i m e : 1 4 : 4 1
:-.-:-=tk Area \fi--r; ; ,-j. 121 Peak Heiqht (ft) : tf. ,-'0£
Background FK Area (ft-s): 0.146 Background Pk Height (ft): 0.745
Blank Corrected Pk ftrea (A-s): 0.121
Concentration (ug/L ) : 10.0
uL dispensed: 5 from 0, 5 fv^om 40, 10 from 2
Replicate 2 (Peak Stored)
Peak flrea (A-s): 0.122
Background Pk Area (ft-s): 0.144
Blank Corrected Pk Area (A-s) : 0. 1£2
Concentration (ug/L ) : 10. 1
Time: 14:44
Peak Height (A): 0.727
Background Pk Height (ft): 0.754
Mean Cone (ug/L ):
10.1
SD: 0.08
RSDC/.): 0. 7b
Standard number 3 applied. C10.03
Correlation coefficient: 0.99902
Slope: 0.0121
fifi
-------
v
-------
Element File: BE.BtL
Date: 09/£0/9S
Data File: EB331.DAT
Technique: HGA
Element: Be
Time: 15:88
ID/Wt File: EB331.IDW
Calib. Type: Linear
Wavelength: £34.9
Slit: 0.70 L
Larno Current : 30
Energy: 60
* '"V A/ Af A* 'V Av A*- A/ A* A* A/ 'V "
Be
ID:
=3. 0ug/L
Seq. No.: 00007
A/S Pos.: 4
Date: 09/£0/
uL dispensed: 5 from 0. 5 from 40, 10 from 4
Reolicate 1 Time: 15:10
Peak Area (A-s): 0.030 Peak Height (A): 0.176
Background Pk Area (A-s): 0.044 Background Pk Height (A): 0. £b0
Blank Corrected Pk Area (A-s): 0.030
Concentration (ug/L ): £.5
uL dispensed: 5 from 0, 5 from 40. IS from 4
Replicate £ (Peak Stored) Time: 15:12
Peak Area (A-s): 0.037 Peak Height (A): 0.£37
Background Pk Area (A-s): 0.05£ Background Pk Height (A): 0. £96
Blank Corrected Pk Area (A-s;: 0.037
Concentration (ug/L ) : 3. 1
Mean Cone (ug/L ): £.3
QC sample is within range £.7 -
SD: 0. 4£
RSD •:•/.) : 15. £7
Be
ID: ICB
Seq. No. : 00003
A/S Pos.: 0
Dats:
uL dispensed: 5 from 0, 5 from 40, 10 from 0
Reolicate 1 Time: 15:15
Peak Area (A-s): 0.000 Peak Height (A): 0.003
Background Pk Area (A-s): 0.005 Background Pk Height (A)
Blank Corrected Pk Area (A-s): 0.000
Concentration (ug/L ): 0.0
uL dispensed: 5 from 0, 5 from 40, 10 from 0
0. 0£
Reolicate £ (Peak Stored)
Peak firea (A-s): 0.000
Background Pk Area (A-s): 0. 00fe
rl^-'l C;- r-5-.-t-2C1 Pk fi>^ea (A-s): 0.000
Conctn b - at i :-n ;..o-i_ •' : 0. C:
Time: IS:17
Peak Height (A): 0.003
Background Pk Height (A)
Mean Cone (uq/L ):
0. 0
SD: 0.01
RSD<%): £4.£1
QC sample is within range -1.0 - 1.0
Be
ID: CHECK LO
Seq. No. : 00009
^ A^ A* A/ *^ A/ ^ A* *V *V A/ *^ A*
A/S Pos. : 6
Date: 09/£0/<
uL dispensed: 5 from 0, 5 from 40, 10 from 6
Replicate 1 Time: 15:£0
Peak Area (A-s): 0.01£ Peak Height (A): 0.030
Background Pk Area (A-s): 0.0££ Background Pk Height : 1.0
uL dispensed: 5 from 0, 5 from 40, 10 from 6
68
-------
^e-plicate £ (Peak Stored) Tine: 15:c:2
:'eak Area (A-s): 0.013 Peak Height (A): 0.064
Background Pk Area (A-s): 0. 0£1 Background Pk Height (A): 0.125
3iank Corrected Pk Area (A-s): 0.013
Doncentrat ion A,'^
3e ID: 46507B MB Seq. No. : 00010 fl/S Pos. : 7 Date: 09/20/98
uL dispensed: 5 from 0. 5 from 40, 10 from 7
Replicate 1 Time: 15:£5
Peak Area (A-s.>: -0.000 Peak Height (ft): 0.003
Background Pk Area (A-e) : 0.005 Background Pk Height (ft): 0.028
Blank Corrected Pk Area (A-s): 0.000
Concentration (uq/L ): 0.0
uL dispensed: 5 from 0. 5 from 40. 10 from 7
Replicate 2 : 0.001
Concentration (ug/L ): 0.1
>1ean Cone (ug/L ): 0.0 SD : 0.06 rtSD>%); 136.64
Be ID: 465S7B LCS X10 Sea. No.: 00G11 ft/5 Pos. : S Date: 09/20/93
uL dispensed: 5 from 0, 5 from 40. 10 from 8
Replicate 1 Time: 15:30
Peak flrea (fl-s): 0.060 Peak Height (ft): 0.400
Background Pk flrea (A-s): 0.080 Background Pk Height (A): 0.430
Blank Corrected Pk flrea (fl-s): 0.060
Concentration (ug/L ): 5.0
uL dispensed: 5 from 0. 5 from 40. IS from 3
Reolicate 2 (Peak Stored) Time: 15:32
Peak flrea : 0.474
Blank Corrected Pk flrea (A-s): 0.064
"*.c~. : c 5 ntrat i on (ug/L ): 5.3
Mean Cone (ug/L '>: 5.1 SD : 0.20 RSDC/.): 3.82
Be ID: 213-12-4 Sea. No. : 00012 A/S Pos. : 9 Date: 09/20/98
uL dispensed: 5 from 0. 5 from 40, 10 from 9
Replicate 1 Time: 15:35
Peak flrea (A-s): 0.025 Peak Height (fl) : 0.048
Background Pk flrea (A-s): 0.110 Background Pk Height (A): 0.183
Blank Corrected Pk Area (A-s): 0.025
Concentration (ug/L ) : 2. 1
uL dispensed! 5 from 0. 5 from 40, 10 from 9
Replicate £ (Peak Stored) Time: 15:37
Peak Area (A-s): i2. 026 Peak Height (A): 0.052
69
-------
-------
-------
Background Pk ftrea Cft-s): 0.113 Background Pk Height (ft): 0.197
Blank Corrected Pk ftrea : 0. 025 Peak Height (ft): 0.055
Backnround Pk ftrea (ft-s): 0.123 Background Pk Height (ft): 0. ££&
Blank Corrected Pk ftrea (ft-s): 0. 0£fc
Concentration (ug/L ) : 2.2
Mean Cone (uq/L ;: 2.2 SD i 0.09 RSD (#) ; 3.97
Be ID: 218-12-10 Sea. No. : 00014 ft/S Pos. : 11 Date: 09/20,
uL disoe-sed: 5 from 0. 5 from 40. 10 from 11
Reclicate 1 Time: 15:44
Peak ftrea (fi-s): 0.025 Peak Height (ft): 0.052
Background Pk ftrea (A-s): 0. 12& Background Pk Height (ft): 0. 2,51
Blank Corrected Pk ftrea (ft-s): 0.025
Concentrabion (ug/L ): 2.0
uL dispensed: 5 front 0. 5 from 40, 10 from 11
Replicate 2 (Peak Stored^ Time: 15:47
Peak ftrea (A-s): i3. ®£5 Peak Height (ft): 0.052
Background Pk ftrea (ft-s): 0.130 Background Pk Height (ft): 0.227
Blank Corrected Pk ftrea (A-s): 0.025
Concentration (ug/'L ) : 2.0
t*ean Cone (ug/L ): c. 0 SD: 01.31 RSDC/O: 0.29
Be ID: 213-12-10 Sep. No.: 00015 ft/S Pos.: 11 Date: 09/20
uL dispensed: 5 from 40, 5 from 2. 10 from 11
Sample abs. is greater than that of the largest standard.
Replicate 1 Time: 15:49
Peak ftrea (ft-s): 0.142 Peak Height (ft): 0.324
Background Pk ftrea (ft-s): 0.268 Background Pk Height (ft): 0.505
Blank Corrected Pk Area (ft-s): 0.142
Concentration (ug/L ): 11.7
uL dispensed: 5 from 40, 5 from 2, 10 from 11
Sample abs. is greater than that of the largest standard.
Replicate 2 (Peak Stored) Time: 15:52
Peak ftrea (ft-s): 0.148 Peak Height (ft): 0.328
-------
background Pk Area (A-s): 0. 27b Background Pk Height (A): 12.545
Hank Corrected Pk Area (A-s) : 0. IAS
Concentration (ug/L ): 12.2
Sample abs. is greater than that of the largest standard.
lean Cone (ug/L ): 12.0 SD: 0.33 RSD (•/.): 3.17
Recovery is 198. 6% (outside of specified limits)
He ID: £18-12-10 D Seq. No.: 00016 ft/S Pos. : 12 Date: 09/20/98
.iL dispensed: 5 from 0, 5 from 40, 10 from 12
Replicate 1 Time: 15:54
:'eak Area (A-s): 0.024 Peak Height (A): 0.044
background Pk Area (A-&>: 0.128 Background Pk Height (A): 0.230
ilank Corrected Pk Area : 1.9
lean Cone (ug/L ); 2.0 SD : 0.05 RSD(5Oj 2.40
»e ID: £18-12-10 MSX10 Sea. No.: 00017 A/3 Pos.: 13 Date: 09/20/9S
.iL dispensed: 5 from 0, 5 from 40, 10 from 13
Replicate 1 Time: 15:59
"-'eak Area (A-s): 0.080 Peak Height (A): 0.208
Background Pk Area (A-s): 0.127 Background Pk Height (A): 0.312
ilank Corrected P'k Area (A-s): 0.080
Concentration (ug/L ): fr.&
.iL disoensed: 5 from 0. 5 from 40. 10 from 13
Reolicate 2 (Peak Stored) Time: 16:02
"'eak firsa (A-s): 0. SSI Peak Heicht (ft): 0. 24f.
"•crl : 0. 129 Background Pk Height (~-^> : C'<. 3^©
^iank Corrected '<-•'- H--ea (A-s): 0.081
joncentrat i on (ug/s_ ): 6.7
lean Cone (ug/L ): 6.6 SD : 0.06 RSDC/4): 0.84
Je ID: 218-12-10MSDX10 Sea. No.: 00018 A/S Pos.: 14 Date: 09/
.iL disoensed: 5 from 0. 5 from 40. 10 from 14
-------
Pe.ak Area (A-s): 0.875 Peak Heiqht (ft): 0.196
Background Pk Area (A-s): 0.122 Background Pk Height (A): 8.£39
Blank Corrected Pk Area (A-s>: 0. 876
Concentration O.ig/L ): 6.2
Mean Cone (ug/L ): 6.2 SB: 0.01 RSDC/.): 0.13
Be ID: CCV=6.Qug/L Seq. No.: 00019 A/S Pos.: 5 Date: 09/20
uL dispensed: 5 from 0. 5 f-rom 40. 10 from 5
Replicate 1 Time: 16:09
Peak Area (A-s): 0.074 Peak Height (A): 0.485
Background Pk Area (A-s): 0.099 Background Pk Height (A): 0.558
Blank Corrected Pk Area (A-s): 0.075
Concentration (uq/L ): 6.2
uL dispensed: 5 from 0, 5 from 40, 10 from 5
Replicate 2 (P'eak Stored) Time: 16:11
Peak Area (A-s): 0.074 Peak Height (A): 0.443
Background Pk Area (A-s): 0.093 Background Pk Height (A): 0.510
Blank Corrected Pk Area (A-s): 0.074
Concentration (ug/L ): 6.1
Mean Cone (ug/L ): 6.1 SD: 0.03 RSD(%): 0. *:
QC sample is within range 4.S - 7.2
Be ID: CCB Sea. No. : 00020 A/3 Pos. : 0 Date-. 09/2'-
uL dispensed: 5 from 0. 5 from 40, 10 from 0
Replicate 1 Time: 16:14
Peak Area (A-s): 0.001 Peak Height (A): 0.004
Background Pk Area (A-s): 0.007 Background Pk Height (A): 0.033
Blank Corrected Pk Area (A-s): 0.001
Concentration (ug/L ): 0.1
uL dispensed: 5 from 0, 5 from 40, 10 from 0
Replicate 2 (P'eak Stored) Time: 16:16
Peak Area (A-s): -0. 000 . F'eak Height (A): 0.004
B = c Unround P'k Area (A-s.-: 0. 0'2'T Backnr-jund Pk He;zht <:H : £, 02^
rluink Corrected Pk Area (A-s>: -0.000
Concentration (ug/L ): -0.0
Mean Cone : 0.005 Peak Height
-------
.»L dispensed : 5 from 0, s from 40, 1
Replicate £ (l-'eak Stored/
:-eak Area (A-s): 0.005
iackground Pk Area (A-s): 0.037
ilank Corrected Pk Area (A-s): 0.005
Concentration (ug/L ): 0.4
-lean Cone ( ug/L ) :
0. 4
from 15
Time: 16:£1
Peak Height (A): 0.011
Background Pk Height (A) :
0. 069
9D: 0.00
RSDC/O : 0.
5e ID: 213-12-10 L
.iL d i spensed : 5
3eol icat e 1
:'eak Area (A-s): 0.000
background Pk Area (A-s): 0.
Mank Corrected Pk Area (A-
"Joncentrat i on (ug/L ) : 0. I/
Seq. /Jo. : 000£2
ft/9 Pos. : 15
Date: 09/20/93
i:, 10
0.001
.iL dispensed: 5 from 4®. p from 2, 10
Replicate £ (Peak Store*
"•'eak Area (A-s) : 0.001
background Pk Area (H-S/ : 0.016
'ilan'-: Corrected Pk Are/ (A-s': 0.002
Concentration (ug/L / 5 0.1
lean Cone (•-tg/L ' / 0. 1
? e c o v e '••'• v is — 3 . 9 "X / 'outside' of s D e c i
from 15
Time: 1&:£3
Peak Height ack aground Pk Area (A-s>: 0.001
ilank/Corrected Pk Area (A-s): -0.000
i on (ug/L ): -0.0
from 5
Time: 16:£3
Peak Height (A): 0.004
Backnround Pk Heiaht (A): 0.00^
from 5
Time: 16:30
Peak Height (A): 0.003
Background Pk Height (A): 0.004
Cone (ug/L ): 0.0
!Csai7iDle is out of range 4.8 - 7.2
SD: 0.0;
RSDC/.) : 215. 70
>t
L
ID: CCB
Seq. No.: 00024
A/S Pos. : 0
Date: 09/20/98
dispensed: 5 from 0, 5 from 40, 10
icat e 1
(A-s): 0.001
Area (A-s): -0. 000
lank Correctd Pk ^i aa — iA-O i — 0.
from 0
Time: 1&:33
Peak Height : 0.006
Backnround Pk Heiaht (A):
0. 004
73
-------
uoncem; rar i on kuo/i_
uL dispensed: 5 from 0, 5 from 40, 10 from 0
Replicate £ (Peak Stored)
Peak Area (A-s): 0.000
Background Pk Area (A-s): 0.001
Blank Corrected Pk Area (A-s): 0.000
Concentration : 30. S£
Be
ID: STD BLANK
Seq. No. : 800£5
0/
A/S Pos.: 0
uL dispensed: 5 from 0, 5 from 40, 10 from
Replicate 1 Time/f 16 : ,
Peak Area (A-s) : 0.001 Peate Height (A.): 0.003
Background Pk Area (A-s): 0.001 Background Pk Height : -K.001 Peak Height (AJ: 0.003
Background Pk Are/
Elani- Corrected yk Area ;A-s): -0.001
0. 00 =
uL dispensed: £i from 0, 5 from 40, 10 from 1
Replicate £ /Peak Stored) Time: 1&:45
Peak Area (AVs): -0.000 Peak Height (A): 0.004
Background Crk Area (A-s): 0.001 Background Pk Height (A): 0.005
Blank Corrected Pk Area (A-s): -0.000
Concentrat/on (ug/L ): —0.0
Mean Cone/ (ug/L ):
-0. 0
SD: 0.82
Be
I
5.0 uq/L
Sea. No. : 000£7
A/S Pos. : 1
RSDC/.) : 59. b"
Date: 09/£0/
uL disoUnsed: 5 from 0. 5 from 40. 10 from 1
ReDlica\e 1 Time: i&:47
Peak AreSsJA-s): 0.000 Peak Height (A): 8.804
-------
ackgroi..nc: Pk Area (A-s): 0.001 Background Pk Height (A;: 0.005
lank Corrected Pk Area (A-s): -0.000
oncentration (ug/L ): -0.0
L disoensed: 5 from 0, 5 from 40, 10 from 1
eoiicate 2 (Peak Stored) Time: 16:49
eak firea (A-s): -0.000 Peak Height (A): 0.003
ackground Pk Area (A-s): 0.001 Background Pk Height (A): 0.005
lank Corrected Pk Area (A-s): -0.000
oncentration (ug/L ): —0.0
ear, Cone (ug/L ): -0.0 ^ ^ RSD ('/.): 105.35
eslope abs. is gr'Srs-rm—Than that of the largest stanoard.
e ID: ICU=3.0ug/L Seq. No.: 00028 fl/j? Pos. : 4 Date: 09/20/96
L disoensed: 5 from 0, 5 from 40, 10 front 4
eclicate 1 Ti:ue:
eak Area (A-s): 0.000 Peak Height (A): 0.005
ackground Pk Area (A-s): 0.001 Sackqy'ound Pk Height (A): 0.004
lank Corrected Pk Area (A-s): 0.000
oncentration (ug/L ): 0.0
L dispensed: 5 from 0, 5 from 40, 10 fr/m 4
eplicate 2 (Peak Stored) Time: 16:54
eak prea (A-s): 3.000 /Peak Height (A'> : 0. 00;
acknround Pk Area (A-sN: 0.001 / Backnrcund Pk Height (A>: 0.004
lank Corrected Pk Area (A-s): 0. 000y
oncent>^at i on (ug/L ) : 0.0
ean Cone (ug/L ): 0.0 / 3D: 0.00 RSD(*>: 4.S3
C sample is out of range
/ _ ^ ^ ^
ID: ICB /Seq. No. : 00029 A/S Pos. : 0 Date: 09/20/98
L dispensed: 5 from 0. 5/Prom 40. 10 from 0
:eolicate 1 / Time: 16:57
ea^ Area ''A-s): 0. 000 / Peak Height. (A): 0.003
• ackcj^o .-.7 d Pk nr- = = 'A-yf; : '3.01?! Backnrour.d PW Heinht (A): i2',0iii4
• lank Corrected Pk A«4a (A-s): 0.000
:oncentrat i on (un/L/): 0.0
iL dispensed: 5 fyom 0, 5 from 40, 10 fv^om 0
!eplicate 2 (Pe/k Stored) Time: 16:59
'eak Area (A-s) / 0. 000 Peak Height (ft): 0.003
lackground Pk /rea (A-s): 0.001 Background Pk Height (A): 0.003
• lank Corr-ect/d Pk Area (A-s): 0.000
!oncentrat i art (ug/L ) : 0.0
lean Cone/ (ug/L ) : 0.0 SD: 0.02 RSDC/): 133.35
!C sample is within range -1.0 - 1.0
>e ID: CCV=6.0ug/L Seq. No.: 08030 A/S Pos.: 5 Date: 09/21/98
75
-------
'_U_ U-i^UJGli'^-eLJi _; ) T 'J III >£.< 4 w 1 I " U' .it "ft.1 « J. M.« I ' 'J 111 w1
Reolicate 1 Time: 06:30
Peak Area (ft-s): 0. (335 Peak Height (ft) : 0. 186
Background Pk Area (A-s): ©.056 Background Pk Height (ft): 0.235
Blank Correct ec Pk Area (ft-si: 0.034
Concentration (ug/L ): 2.8
uL dispensed: 5 from 0, 5 from 40, 10 from 5
Replicate 2 (Peak Stored) Time: 06:33
Peak Area (A-s): 0.061 Peak Heiqht (ft): 0.325
Background Pk Area (A-s) : 0.092 Background Pk Heiqht (ft): 0.434
Blank Corrected Pk Area (ft-s): 0.061
Concentration (ug/L ): 5.0
Mean Cone (ug/L ): 3.9 SD: 1.57 RSD(%): 39. '/I
Be ID: CCV=6.0ug/L Seq. No.: 00031 ft/S Pos.: 5 Date: 09/21/9,
uL disoensed: 5 from 0, 5 from 40, 10 from 5
Be ID: CCY=6.0ug/L Sec. No.: 00032 A/S Pos.: 5 Date: 09/21,-9
uL dispensed: 5 from 0. 5 from 40, 10 from 5
Radicate 1 Time: 07:06
Peak ftrea (ft-s.>: 0.060 Peak Height (ft): 0.296
Background Px ftrea (A-s) : 0. 09S Background Pk Heiqht (ft.- : 0.380
Blank Corrected Pk Area (ft-s>: 0.060
Concentration (uq/L ): 5.0
uL dispensed: 5 from 0, 5 from 40, 10 fr^om 5
Replicate £ (Peak Stored) Time: 07:09
Peak ftrea (A-s): 0.063 Peak Height (ft): 0.344
Background Pk Area (fl-s): 0.093 Background Pk Height (ft): 0. 39C-
Blank Corrected Pk Area (A-s): 0.063
Concentration (un/L ): 5.2
Mean Cone (ug/L ): 5.1 9D: 0.17 RSDC/.): 3.24
QC sample is within ranqe 4.3 - 7.2
Be ID: 1>I£ Sec. Nc.1 00033 A/3 Pos.: 0 Date: 09/i=:l/{
uL dispensed: 5 f-rom 0, 5 from 40, 10 from 0
Reolicate 1 Time: 07:11
Peak flrea (A-s): 0.001 Peak Height (ft): 0.004
Background Pk Area (A-s): 0.009 Background Pk Height (A): 0.040
Blank Corrected Pk Area (A-s): 0.001
Concentration (ug/L ) : 0. 1
uL dispensed: 5 from 0, 5 from 40, 10 from 0
Replicate 2 (Peak Stored) Time: 07:14
Peak Area (A-s): 0.001 Peak Height (A): 0.004
Background Pk Area (A-s): 0.008 Background Pk Height (ft): 0.033
Blank Corrected Pk Area (ft-s): 0.001
Concentration (ug/L ): 0.1
Mean Cone (ug/L ): 0.1 SD: 0.02 RSDC/4): 22.82
76
-------
3C. samcle is wit run ranqe -1.0 - 1.0
ID: CHECK LO
Sec. No. : 00034 A/S Pos. : b
Date: 89/21/98
.iL disoensed: D from 0, 5 from 40, 1
3eplicat e 1
-'eak Area (A-s): 0.011
Background Pk Area (A-9>: 0. 0£&
Jlank Corrected Pk Area (A-s): 3.011
Concentration (un/L ): 0.9
from fr
Time: 07:lb
Peak Height (d) : 0. 0&£
Background P/ Height (A): 0.11&
AL dispensed: 5 from 0, 5 from 40, 10
Replicate £ (Peak Stored)
:: 0/009
Jlank Corrected Pk Area (AVs): -0.000
Concentration (uq/L ) : -Cr. 0
from 7
Tine: 07:£1
Peak Height (A1: 0.003
Background Pk Height (A):
• r o m /
Time: 07: £4
Peak Height (A): 0.003
Background Pk Height (A't :
0. 03
0.0;
lean Cone (ug/L ) :
-0. 0
SD: 0.
RSDC/.) : £09.06
ID: 4o507B L.CS /10
Sea. No.
iL dispensed: 5 fro!/ 0. 5 from 40. 10
?epl icat e 1
^'eak Area (A-s*: 0/055
iackground Pk AreA (A-s): 0. 0S3
Hank Corrected /k Area (A-s): 0.054
Concentration (yfg/L ) : 4.5
.iL disoensed : /ii from 0, 5 from 40. 10
-------
X- -"V- -X- •'X' -X -X- •"-• "w ~w •"*-• -X- -"V -X/ -"V -X? -"V -X- 'w- -XT -"V -X- X- *>»• "w "Vr -X- -V -"V -X- Ac -X- -\f -X- V -X- -X -X- -"V -"
B 3
ID: £18-1£-4
Sea. No.: 00037
f -X- 'V -X X- -~j J
ft/S Pos.
•jL disoensed: 5 from 0. 5 from 40.
Repi icat e 1
Peak HY-ea (fi-s1): 0.
Background Pk fir&H ft-s) : 0. 135
Blank Corrected Pk Area (A-s): 0. <3£5
Concentration (ug/L ): £.1
Time: 07:31
Peak Height (ft^: 0.053
Background P Height
uL discensed: 5 from 0. 5 from 40. 10 from 9
Reolicate £ (Peak Stored)
Peak Area (A-s): 0. i3£7
Background Pk Area (A-s) : 0. 13£
Blank Corrected F'k Arsa :
Background Pk Are(A-s): 0.135
Blank Corrected Q£ Area (A-s): 0.0£&
Concentration (!/c/L ) : £.1
Mean Cone (ua/L ):
£. 1
Time: 07:3&
Peak Height : 0.05-
Background Pk Height (A)
f r o m 10
Time: 07:33
Peak Heioht (H): 0.054
Backaround Pk Heiqht (A)
Dats:
: 0. £££
SD : 0. 0£
RSD ','/.
1.0:
Be ID: 31 3-1 £-10
uL d ". s c-ened: 5 F--C
Sea. No. : 00039
0. -I f-orp 40. '0 from 1 1
A/S Pos. : 11
Date: 09/21
-------
Is,-nen 1- File: BtMSP.bE
lament: Be
vint Data: Main+SuDDl.
rint: Calib. Curve
Analyst: BENNETT
Peak Storaae: 1 Reel./Sample
INSTRUMENT: 410® 2L
avelenqth: £34.9 Peak
agnal Type: Zeeman AA
ead Time: 3.0
ample Replicates: 2.
tandard Replicates: £
Technique: HGA Version: 7. 3<3
SI it: 0.7 Low
Signal Measurement: Peak Area
Read Delay: 0.8 BUG Time: 2.
Spike Replicates: Same as Sample
AL I BRAT I ON:
So lut ions
_1'L_ C 1 — i- \ i
a i i o. b 1 =in K
tandard 1
tandard £
T
1 ID i Cone
1 !
,-.—.-_ — . — . .., .
I £N 1 U 13 L_ H p4 r\ I
!STD1= 5 ug/L ! 5. 0
ISTD£= 10 ug/L ! 10.0
r ]
Locat i on
P.
**•'
i
£
Vol ume
1 1"^
i V.1
10
10
1 i?
Diluent
Vc 1 ume
i •'i
i «.<
1 1 !7l
Mod i f i er 1
#1 1 ttS i
cr I I
H> 1 f
5 1 i
5 1 t
er i i
Diluent Location: 0
Modifier 1*1 Location: 40
Calibration Units: ug/L
Calibration Tyoe: Method of Add.
Modifier #£ Location
Sample Units: ug/L
urn ace lime/Temperature Program:
t e p
1
£
3
4
5
n j e
i """ e m D
1 1 1'Zi
1 133
i 1500
! £300
1 £500
ct ion
R a m D
i
1
Zf
0
1
Temp
Hold
i^' ^'
£0
15
i^1
5
: £0
1 G&s F 1 3 w i ri e a d
i £50 !
! £50 !
! £50 i
i 0 1 *
i £50 !
Pi pett e
i Gas i voe '
i !"4 o r m i
1 Norm !
i Norm !
1 N o r m !
1 Norm 1
Speed: £5"4
Extraction Svstem: Off
EDUENCE:
tep fiction and Parameters
1 Pioet diluent -t- modifier 1 + spike
£ Run HGft stsos 1 to End
3 Extra washes: 1
sample/std
HECKS 5
dditiins r'-^epa>"at i on : Automated
p '"• i c U i z £'' *~ o r = -••;? L' c ~ t i r : P .1 * 3's m p 1 =?«
f '/.RSD > £0.0 and Concentration > 1.0
heck J4RSD on: Samples + Additions
then Retry 1 times
C:
atrix Check Calculations:
Difference for Duols: No
Recovery for Spike: No
Locat ions:
Locat i ons;
Cone;
79
-------
Element File: Bt'MSA. GEL Element: Be Wavelength: £34.9
Date: 09/£l/98 Time: 07:53 Slit: 0. 7 L
Data File: EB331.DAT ID/Wt File: EB331.IDW Lamp Current: 30
Technique: HGA Calib. Tvpe: Method of Add. Energy: S4
* A/ A/ A* *V A/ A/ A/ A* A*
Be ID: STD BLANK Seq. No. : 00040 A/3 Pos. : 0 Date:
uL dispensed: 10 from 0, 5 from 40. 10 from 0
Replicate 1 Time: 07:55
Peak Area : ^ Data: 09/£l-'9£
uL dispensed: 10 from 0, 5 from 40, 10 from 9
Replicate 1 Tims: 08 : OO
Peak Area (A-s): 0. 3£3 Peak Height (A): 0.045
Background Pk Area (A-s): 0.129 Background Pk Height (A-: 0. .= '36
Blank Corrected Pk Area (A-s): 0. 0£3
uL dispensed: 10 from 0, 5 from 40, 10 from 9
Reolicate £ (Peak Stored) Time: 08:03
Peak Area (A-s): 0. 3£4 Peak Height (A): 0.045
Background Pk Area (A-s): 0.130 Background Pk Height (A): 0. £15
Blank Corrected Pk Area (A-s): 0. 0£4
We^n Pk Area (A-s^: 0. 0£4 SD : 0. 000fr R'dDCV." s £.58
ID: 5'"C1- '-• uq/L Seq, No.: 0004£ A/S Pos.: 9 Oat s : 09/£l/9.
uL dispensed: 5 from 40, 10 from 1, 10 from 9
Replicate 1 Time: 08:05
Peak Area (A-s): 0.130 Peak Height (A): 0. £9S
Background Pk Area (A-s): 0. £65 Background Pk Height (A): 0.508
Blank Corrected Pk Area (A-s) : 0. 131
uL dispensed: 5 from 40, 10 from 1. 10 from 9
Replicate £ (Peak Stored) Time: 08:08
Peak Area (A-s): 0.131 Peak Height (A): 0. £99
Background Pk Area (A-s): 0. £65 Background Pk Height (A): 0.509
Blank Corrected Pk Area (A-s) : 0. 131
Mean Pk Area
-------
.tl_' dispensed: 5 from 40. 13 from 2. 10 f>-om 9
Replicate 1 Time: 08:11
:'eak Area (A-s): 0.231 Peak Height (A): '3.487
Background Pk Area ncentrotlon
10.0
Be
ID: STD BLANK
Sea. No.: 00044
A/S Pos.: 0
Date: 09/21/9S
uL dispensed: 10 from 0, 5 from 40, 10 from 0
Replicate 1 Time: 08:17
Peak Area (A-s): 0.000 Peak Height (A): 0.003
Background Pk Area (A-s): 0.009 Background Pk Height (A): 0.033
Blank Corrected Pk Area (A-s): 0.000
uL dispensed: 10 from 0, 5 from 40, 10 from 0
Replicate £ (Peak Stored) Time: 08:19
Peak Area (A-s): -0.000 Peak Height
-------
Auto — zero performed.
Be ID: £18-12-7 Sea. No.: 00045 A/S Pos. : 10 Date: 09/21/98
uL disoensed: IS from 0, 5 from 40, 10 from 10
Replicate 1 Time: 03:££
Peak Area (A-s): 0.023 Peak Height D <•/•>: 0.49
Be ID: STD1 = 5 ug/L Seq. No.: 00046 A/S Pos.: 10 Date: 09/21/9J
uL dispensed: 5 from 40, 10 from 1, 10 from 10
Replicate 1 Time: 08:28
Peak Area (A-s): 0.123 Peak Height i Backnround Pk Hainht : 0. 268 Background Pk Height (A): 0. 486
Blank Corrected Pk Area ^<=3 .ft-s); -3. £32
uL dispensed: 5 from 40, 10 from 2, 10 from 10
Replicate £ (Peak Stored) Time: 06:36
Peak Area (A-s): 0.230 Peak Height (A): 0.497
Background Pk Area (A-s): 0.384 Background Pk Height (A): 0.656
Blank Corrected Pk Area
-------
i {Display Calibration - C;\flflj
o.aat-.
t
-1.1
Concentration
to.fl
ID: 5TD BLANK
&2C. No. : 03S4B
ft/3 Pos.: 0
Date: 09/21/98
uL dispensed: 10 frora 0. 5 from 40. 10 from 0
Replicate 1 Time: 03:39
Peak Area (ft-s): 0.001 Peak height (rt): 0.004
Background Pk ftrea : 0.001 Peak Height (A): 0.003
Background Pk Area (A-s): 0.007 Background Pk Height (ft): 0.022
Blank Corrected Pk ftrea (ft-s): 0.001
Mean Pk ft^ea >'A— s, :
h "j * "—?=•,- o r> e r f o r in & d.
0. 001
SD: 0. 0002
RSD C/..' :
Be
ID: £18-12-10
Sea. No.: 00049
ft/S Pos.: 11
Dat?:
uL dispensed: 12i from 0, 5 from 40, 10 from 11
Replicate 1 Time: 08:44
Peak Area (A-s): 0.021 Peak Height (A): 0.038
Background Pk Area (A-s): 0.138 Background Pk Height (ft): 0. ££4
Blank Corrected Pk ftrea (ft-s): 0.021
uL dispensed: 10 from 0, 5 from 40, 10 from 11
Replicate 2 (Peak Stored) Time: 08:47
Peak ftrea (A-s): 0.022 Peak Height
-------
uL' dispensed: 5 from 40. 10 from
Re pi icat e 1
Peak Area : 0.120
Background Pk Area : 0.119
Be ID: STD2= 10 ug/L Sep.
uL disoensed: 5 from 40. 10 from
ReDlicate 1
Peak Area
-------
e ID: STD BLANK Sea. No.: 00052 A/S Pos. : 0 Date: 09/21/93
L dispensed: 10 from 0, 5 from 40, 10 from 0
eplicate 1 Time: 09:01
eak Area (A-s): 0.001 Peak Height (ft): 0.004
ackground Pk Area (A-s): 0.007 Background Pk Height (A): 0.019
lank Corrected Pk Area (A-s): 0.000
L dispensed: 10 from 0, 5 from 40, 10 from 0
ieolicate 2 (Peak Stored) Time: 09:04
'eak firea : 0.000 Peak Height (A): 0.003
Background Pk Area (A-s): 0.006 Background Pk Height (A): 0.018
• lank Corrected Pk Area (A-s): -0.000
lean Pk Area (A-s): -0.000 SD : 0.0003 RSDC/O: 629.97
tuto — zero performed.
's -D: 213-12-10 D Sea. No.: 00053 A'S Pos.: 12 Dat ? : 09/2i,'93
.L d i = oensed : 10 from 0, 5 from 40, IS fr^rs 12
I e D 1 i cat e 1 T i m e : 09 : 06
'eak Area (A-s.): 0.020 Peak Height (A): 0.036
Background Pk Area (A-s>: 0.141 Background nk Height (A): 0.230
ilank Corrected Pk Area (A-s): 0.019
tL dispensed: 10 fro a 0, 5 from 40, 10 from 12
ieolicabe 2 (Peak Stored) Time: 09:09
:'eak Area (A-s): 0.020 Peak Height (A): 0.036
'ackg'-ound Pk Area (A-s): 0.1^2 Background Pk Height (A): 0.217
Mank Corrected Pk Area : 0.019 SD : 0.0001 RSDC/.j; 0.69
ie ID: STDl- 5 ug/L Seq. No.: 00054 A/£ Pos.: 12 Date: 09/21/95
iL dispensed: 5 from 40, 10 from 1, 10 from 12
Replicate 1 Time: 09:12
:'e«k Are- a (A--': 0,118 Peak Height (A): 0.234
*=li -' : - " - °u ^'"tra (P,-s,- ; 0.269 Backnround Pk Height (ft.) : 0. 4£.£
Jlank •Lorrected Pk Area (P-si; 0.117
.(L dispensed: 5 from 40. 10 from 1. 10 from 12
^eolicate 2 (Peak Stored) Time: 09:15
:'eak Area (A-s): 0.120 Peak Height (A): 0.241
Background Pk Area (A-s): 0.274 Background Pk Height (A): 0.434
31ank Corrected Pk Area (A-s): 0.119
lean Pk Area (A-s): 0.113 SD : 0.0017 RSD(5O: 1.48
3e ID: STD2= 10 ug/L Sea. No. : 00055 A/S Pos. : 12 Date: 09/21/93
.iL dispensed: 5 from 40, 10 from 2. 10 from 12
Replicate 1 Time: 09:17
:-eak Area (A-s): 0.212 Peak Height : 0.435
background Pk Area (A-s): 0.378 Background Pk Height (A): 0.616
31ank Corrected Pk Area (A-s): 0.211
85
-------
uL dispensed: 5 from 40, 10 from 2, 10 from i£
Replicate £ (Peak Stored) Time: 09: £0
Peak Area (A-s): 0. £29 Peak Height (A): 0. 44?
Background Pk Area (A-s): 0.394 Background Pk Height (ft): O.&ll
Blank Corrected Pk Area Cft-s): 0.223
0. ££0
Mean Pk ftrea (fl-s):
Be ID: £13-12-10 D
Concentration (ug/L ): 1.0
Correlation coefficient: 0.99935
SD: 0.012
Seq. No.: 00053
ft/S Pos. : 12
RSDC/O : 5. 43
Date:
Slope: 0. 0£00
^{Display Calibratifll! - C.1 \ftft
86
-------
sUht Pile: AB93S.IDK Analyst: D.STREETER-EDIARDS
le »oluie: 100 iL loiiial Height: 1.0 g
:. Saiple ID Height Dilation
0
1
2
3
4
5
6
7
8
9
0
1
2
3
4
5
6
7
8
9
0
1
2
3
4
5
6
7
8
9
0
1
2
3
4
r
!6
17
18
19
10
•1
i2
3
!4
*
16
•7
,8
13
STD BLA8[ •->
STDl=0.2ug/l
5TD2=Q,5ug/L
STD3=1.0ug/L
STD4=2.0ng/L
STD5=5.Q*g/l
STD6=10.0ag/L(
lC?=4,Oug/L -
ICB
CHECK LO
46705B KB
46705B UBD
46705B LCS
46705B ICSD
218-12-4
218-12-4 D
218-12-4 KS
218-12-4 KSC
CCVl=6.0u?/L
CCB
218-12-?
218-12-? D
218-12-10
218-12-10 D
CCV2:6.0u?/L
CHE
467Q5A KB
46705A RED
I6705A LCS
46705A LCSD
218-12-1
218-12-1 D
218-12-3
218-12-3 D
218-12-3 US
218-12-3 USD
CCVl=6.0ug/L
CCB
218-12-2
218-12-2 D
218-12-5
218-12-5 D
218-12-8
218-12-8 D
218-12-6
218-12-6 D
218-12-9
218-12-9 D
CC72=6. dag/1
CCB
V
)
\ A W
M-7(D-£
i
\
)
^- 3-^-5 T
— ' u ~* r)t) '5i 1
/ i 1^ ^x ^^i
• !• ^ ^^ •*• i 1 1 ^ | I
'
3- no -5,1
~Tr\*~ Ci ~1
f ^ Or— LP O} '
^
87
-------
Sleient File: 5G..HEL
Eleient: Eg
Print Data: KaintSuppl.
Print: Calib. Curve
Remits:
STASDARDS: SPEI 3-70-6,8
DC: HIGH PORITY 3-70-5,7
IHSTROKEiT: 5100
iaielength: 253.7 Peak
Signal Type: AA
Sead Tiie: 30.0
Saiple Replicates: 1
Standard Replicates: 1
Analyst: ED1ARDS
Peak Storage: Dote
Technique: KHS Version: 7.01
Slit: 0.70 Lot
Sigial Xemreieit: Peak Height (!)
Read Delay: 0.5 BOC Tiie: 2
FLAKE:
Flaie Type: Air
Oxidant Flov: 10.0 L/iin
CAIIBRATIOR:
Solutions ! ID
i
fal iK BUnlr 'QTH Rtf
oaiiD. tuauK |jiu on
Standard 1 !STD 1
Standard 2 |STD 2
Standard 3 ,'STD 3
Standard I ISTD <
Standard 5 |STD 5
Standard 6 ISTD 6
Calibration Onits: ug/L
Calibration Type: Linear
QC:
Ratrii Check Calculations:
1 Difference for Dupls: Ho
I Recovery for Spike: do
Plate
Fuel 1
COBC
0.200
0.500
1.000
2.000
5.000
10.000
Saipl
Locations:
Locations:
Sensor: On
'lor. 2.0 L/iin
'. Units: sg/L
Cone:
-------
tent File: EG .MEL Eleient: Eg »a?eiength: 253.7
;: 09/22/98 Tiie: 13:(S Slit: 0.70 L
i File: AB936.DAT ID/it Pile: AB936.IDK Laip Current: 0
uique: KHS Calib. Type: Linear Energy: 74
uk 1: STABDARDS: SIEI 3-70-6,8
irk 2: QC: EIGH POEITY 3-70-5,7
ID: 5eq. 00035 5eq. So.: 00035 A/S Pos.: -- Date: 09/22/98
licate 1 Tiie: 14:32
i Area li-»): 0.011 Peak Beigkt (A): -0.002
ik Corrected Pk Eeijkt (A): -0.002
:entratioa lag/I |: -O.Q22
i-zero perfoned.
ID: Seq. 00036 Seq. io.: 00036 A/S Pos.: -- Bate: 09/22/9F
licaw 1 Tiie: 14:33
i Area (A-si: -0.031 Peak Height (A): -0.002
ak Corrected Pk Height !A|: -0.002
:eatratioa (ug/l I: -0.025
j-zero perfoned.
8.9
-------
Eleient File: HG .XEl Eleient: Bg lavelength: 253.?
Date: 09/22/98 Tiie: 14:34 Slit: 0.70 I
Data Pile: AB936.DAT ID/HI File: AB936.IDI lup Cureit: 0
Technique: K8S Calib, Type: linear Energy: 75
Reiark 1: STASDABDS: SFEI 3-70-6,8
Seiark 2: QC: HIGH PBRITY 3-70-5,7
Hg ID: STD BLASE Seq. Bo.: 00037 A/S FOE.: -- Date: 09/22/98
Replicate 1 Tiie: 14:35
Peak Area (A-sh -0.019 Peak Height (A): 0.000
Blank Corrected Pk Height (A): 0.000
Concentration (ug/l ): 0.000
Auto-sero perfoned.
Eg ID: STDl=0,2ug/l Seq. lo.: 00038 A/S Pos.: -- Date: 09/22/9E
Jeplicite 1 Tiie: 14:36
Peak Area (A-s): 0.056 Peak Beigkt (A): 0.004
Blank Corrected Pk Height (A|: 0.004
Concentration (ug/l |: 0.058
Standard amber 1 applied. [0,200)
Correlation coefficient: 1.00000 Slope: 0.0196
Hg IB: ST»2-0.5ag/[, Seq. So.: 00039 A/S Pos.: -- Date: 09/22/9E
Saiple abs. is greater than that of the largest standard.
Replicate 1 Tiie: 14:37
Peak Area (A-s): 0.259 Peak Height (A): 0.016
Blank Corrected Pk Height (A): 0,016
Concentration lag/I ): 0.795
Standard nuiber 2 applied. [0.500]
Correlation coefficient: 0.94072 Slope: 0.0300
Hg ID: STD3=1.0ng/l Seq. So.: 00040 A/S Pos.: -- Date: 09/22/98
Saiple abs. is greater than that of the largest standard.
Replicate 1 Tiie: 14:38
Peak Area (A-s): 0.605 Peak Height (A): 0.036
Blank Corrected Pk Height (A): 0.036
Concentration (ug/l ): 1.189
Standard umber 3 applied. [l.OOOj
Correlation coefficient: 0.98278 Slope: 0.0346
Bg ID: STD4=2.0ng/l Seq. So.: 00041 A/S Pos.: - Date: 09/22/91!
Saiple abs. is greater than that of the largest standard.
Eeplicate 1 Tiie: 14:39
Peak Area (A-s): 1.235 Peak Height (A): 0.072
-------
ik Corrected Pk Height (A): 0.072
centratton I tig/1 ): 2.084
indard nuber 4 applied. [2.000]
•relation coefficient: 0.99658 Slope: 0.035?
ID: STD5s$.On/l Seq. Jo.:
1/3 Pos.: -- Hate: 09/22/98
iple abs. is greater than that of the largest standard.
ilicate 1 Tiie: 14:40
ik Area (A-s): 3.140 Peak Height (A): 0.198
ink Corrected Pk Height (A): 0.198
icentration (ug/L ): 5.532
indard umber 5 applied. [5.000]
•relation coefficient: 0.99820 Slope: 0.0389
jlicate 1
ak Area (A-s)
ink Corrected
ncentration (
Slope: 0.0333
ID: STD6=10.0u?/l Seq. So.:
A/SPos.:-- Date: 09/22/98
iple abs. is greater than that of the largest standard.
plicate 1 TUe; U:48
ak Area (A-sj: 6.321 Peak Height (A): 0.389
ank Corrected Pk Height (A): 0.389
ncentration (ug/l ): 11.673
andard amber 5 applied. [10.000]
rrelation coefficient: 0.99962 Slope: 0.0388
91
-------
Eleient File: EG..KEL Eleient: Eg
Date: 09/22/98 Tiie: 14:49
Data Pile: AB936.DAT ID/It File: AB936.IDI
Technique: IBS Calib. Type: linear
Reiark 1: STARDARDS: SPEI 3-70-6,9
Reiark 2: QC: BIGB PORITY 3-70-5,7
lavelengta: 253.
Slit: 0.70 t
laip Current: 0
Energy: 75
7
H
Display Calibration - C:\flftJSER\flfl_FILES\ELEMEHT\HG_.HEL
Linear
Corn. Coef.: 8.99962
Slope; B.B389
Concentration
10.
Eg ID: ICV=4.0ng/l Sec. h.:
A/S Pos.: -- Date: Q9/22/9F
Replicate 1 Tiie: 14:51
Peak Area (A-s): 2.327 Peak Eeigkt (A): 0.1(1
Blank Corrected Pk Height (A): 0.141
Concentration (tg/L ): 3.638
Eg ID: ICE
Seq. io.:
Replicate 1
Peak Area (A-s): -0.118
Blank Corrected Pk Height (A): -0,C
Coiceitratioi (ug/L ): -0.124
i/S Pos.: - D*te: 09/22/9P
Tiie: 14:53
Peak Height Ui: -0,0
Eg ID: CEECK 10
Seq, Io.: 00047 A/S Pos.: - Date: 09/22/98
Replicate 1 Tiie: 14:54
Peak Area (A-s): 0.009 Peak Beignt (A): O.fl
k R»i
-------
lent File: HG .KEL
3: 09/22/98
i File: AB936.DAT
Unique: KHS
Eleient: Eg
Tiie: 14:55
IB/it Pile: AB936.IDI
Calib. Type: Linear
lavelength: 253.'
Slit: 0.70 L
lup Current: 0
Energy: 75
irk 1: STA8DARDS: SPEI 3-70-6,8
irk 2: QC: HIGH POBITY 3-70-5,7
ID: 46705B KB
Seq. lo.
A/S Pos.: - Date: 09/22/9F
licate 1
k Area (A-g): 0.027
ok Corrected Pk Height (A): O.C
centratioa (ig/l ): 0.039
Tiie: 14:55
Peak Height (A): 0.
ID: 46705B KBD
Seq. io.
A/S Pos.:-- Date: 09/22/9F
licate 1
k Area (A-s): 0.017
ilk Corrected Pk Height |A): O.
centration Ug/L |: 0.021
Tiie: 14:56
Peak Height (A): 0.
licate 1
.k Area (A-s
,nk Corrected
,ce
ID: 46705B LCS
Seq, lo.:
A/S Pos.: -- Date: 09/22/9F
ilicate 1
ik Area (A-s]: 2.978
ink Corrected Pk Height (A): 0,179
icentration lug/L ): 4.596
Tiie: 15:02
Peak Height (A): 0.179
ID: 46705B LCSD
Seq. lo.:
A/S Pos.: - Date: Q9/22/9F
plicate 1
ik Area (A-s): 3.020
ink Corrected Pk Height (A): 0.193
icentration Ug/L ): 4.962
Tiie: 15:03
Peak Jeight (A): 0.193
ID: 218-12-4
Seq. Ho.:
A/S Pos.
Date: 09/22/9F
plicate 1
ik Area (A-sl: 0.079
aak Corrected Pk Height (A): 0.
ncentration Ug/l ): 0.114
Tiie: 15:04
Peak Height (Aj:
ID: 218-12-4 D
Seq. lo.: 00054 A/S Pos.
Date: 09/22/9F
-------
epiicate 1
eak Area (A-s): 0.012
lank Corrected Pk Height (A): fl.C
onceutration lug/I 1: 0.010
Tiie; 15:05
Peak Height (A): 0.0
t ID: 218-12-4 KS
Sea. So.:
A/SPOB.:-- Date: 09/22/98
.epiicate 1
Jeak Area (A-sl: 2.838
ilank Corrected Pk Height (A): 0.16?
loficeatration ing/L ): 4.286
Tiie: 15:06
Peak Height JA): 0.16?
ig ID: 218-12-4 USD Seq. So.:
Jepiicate 1
"Jeak Area (A-s): 2.783
Blank Corrected Pk Height (A): 0.166
Concentration (ug/L ): 4,271
A/SPos.:-- Date: 09/22/95
Tiie: 15:0?
Peak Height (A): 0.166
Jg ID: CCVl=6.0ug/L Seq. Bo.:
Jepiicate 1
Peak Area (A-si: 3.500
Blank Corrected Pk Height (A): 0.221
Concentration {ug/L ): 5.690
A/S Pos.: -- Date: 09/22/98
Tiie: 15:08
Peak Height (A): 0.221
Hg ID: CCB
Seq. So.
A/S Pos.: -- Date: 09/22/98
Replicate 1
Peak Area (A-s): 0.002
Blank Corrected Pk Height (A): -0.0
Coacentratiot (ug/L ): -0.008
Tiie: 15:09
Peak Height (A): -0.0
Replicate 1
Peak Area lA-s): 0.131
Blank Corrected Pk Height (A): 0.021
Concentration (ug/L 1: 0.532
Tiie: 15:09
Peak Height (Ai
So.: 00060 A/S PC
Seplicate 1
Peak Area (A-
Blank
Kg ID: 218-12-10
Seq. So.: 00061 A/S Pos.: -- Date: 09/22/98
Replicate 1
Peak Area (A-s): 0.190
Blank Corrected Pk Height (A): 0.010
Tiie: 15:12
Peak Height U): 0.010
f\ A
-------
loncentration (ug/L ): 0.266
[g ID: 218-12-10 D Seq. So,: 00062 A/S Pos.: -- Date: 09/22/38
leplicate 1 Tiie: 15:14
'eakArea (A-s): 0.210 Peak Height (A): 0.012
Uaak Corrected Pk Height (A): 0.012
!oncentration (ug/L ): 0,315
Ig ID: 218-12-? Seq. So.: 00063 A/S Pos.: -- Date: 09/22/98
iepiicate 1 Tiie: 15:15
'eak Area (A-s): 0.182 Peak Height (A): 0.010
ilank Corrected Pk Height (A|: 0,010
loncentration (ug/L ): 0.253
Ig ID: 218-12-7 D Seq. So.: 0006* A/S Pos.: -- Date: 09/22/98
Jepiicate 1 Ttie: 15:16
Peak Area (A-s): 0.196 Peak Height (A): 0,012
Blank Corrected Pk Height (Al: 0.012
^oncentration (ug/L ): 0,302
i<-
implicate 1
Peak Area (A-sh 4.925
Blank Corrected Pk Hei
Hg ID: CCV2:6.0ug/l Seq. So.: 00066 A/S Pos.: -- Date: 09/22/98
Replicate 1 Tiie: 15:21
Peak Area (A-si: 3.551 Peak Height (A): 0.216
5ian'< Corrected P." Height !A|: 0.216
Concentration ug/l !: 5.554
Ig ID: CCB Seq. So.: 0006? A/S Pos.: -- Date: 09/22/98
Seplicate 1 Tiie: 15:22
Peak Area (A-s|: 0.008 Peak Height (A): -0.001
Blank Corrected Pk Height (A): -0.001
Concentration Ug/l ): -0.015
3*
-------
TECHNICAL REPORT DATA
Please read instructions on the reverse before completing
1. REPORT NO.
EPA-454/R-00-025B
2.
4. TITLE AND SUBTITLE
Final Report
Hot Mix Asphalt Plants,
Truck Loading and Silo Filling,
Manual Methods Testing,
Asphalt Plant C,
Los Angeles, California
Volume 2 of 8
7. AUTHOR(S)
Frank J. Phoenix
9. PERFORMING ORGANIZATION NAME AND ADDRESS
Pacific Environmental Services, Inc.
Post Office Box 12077
Research Triangle Park, North Carolina 27709-2077
12. SPONSORING AGENCY NAME AND ADDRESS
U.S. Environmental Protection Agency
Office of Air Quality Planning and Standards
Emissions, Monitoring and Analysis Division
Research Triangle Park, North Carolina 2771 1
3. RECIPIENT'S ACCESSION NO.
5. REPORT DATE
May 2000
6. PERFORMING ORGANIZATION CODE
8. PERFORMING ORGANIZATION REPORT NO.
10. PROGRAM ELEMENT NO.
11. CONTRACT/GRANT NO.
68-D-98004
13. TYPE OF REPORT AND PERIOD COVERED
Final
14. SPONSORING AGENCY CODE
EPA/200/04
15. SUPPLEMENTARY NOTES
16. ABSTRACT
The United States Environmental Protection Agency (EPA) Office of Air Quality Planning and Standards (OAQPS) is investigating hot mix
asphalt plants to identify and quantify paniculate matter (PM), methylene chloride extractable matter (MCEM), and organic hazardous air pollutant
(HAP) emissions during asphalt concrete loading operations. In support of this investigation, the OAQPS issued Pacific Environmental Services. Inc
(PES) a series of work assignments to conduct emissions testing at a hot mix asphalt plant during load-out operations.
The primary objective of the emissions testing was to characterize the uncontrolled emissions of PM, MCEM, polynuclear aromatic hydrocarbons
(PAHs), semi-volatile organic hazardous air pollutants (SVOHAPS), and volatile organic hazardous air pollutants (VOHAPS) from a box mix
production plant during loading operations. An asphalt plant south of Los Angeles, California was selected by EPA as the host facility. Testing
was performed over five consecutive days beginning on July 24, 1998. Testing was performed under two conditions. Under normal operations, testing
was performed to characterize load-out emissions from the tunnel exhaust and load-in emissions from the asphalt concrete storage silo. Under
background conditions, testing was performed to characterize emissions from the combustion of diesel fuel in transport trucks.
The entire report consists of eight volumes totaling 4,234 pages, Vol. 1 (388 pages), Vol. 2 (308 pages), Vol. 3 (573 pages), Vol. 4 (694 pages),
Vol. 5 (606 pages), Vol. 6 (564 pages), Vol. 7 (570 pages), and Vol. 8 (531 pages).
17.
a. DESCRIPTIONS
Hazardous Air Pollutants
Methylene Chloride Extractable
Matter
Paniculate Matter
Polynuclear Aromatic Hydrocarbons
Semi-volatile Organic Hazardous Air
Pollutants
Volatile Organic Hazardous Air
Pollutants
18. DISTRIBUTION STATEMENT
Unlimited
KEY WORDS AND DOCUMENT ANALYSIS
b. IDENTIFIERS/OPEN ENDED TERMS
19. SECURITY CLASS (This Report) *
Unclassified ,
20. SECURITY CLASS (This page)
Unclassified
c. COASTI Field/Group
21. NO. OF PAGES
^ i .Vol. 2r308,r . •".
22. PRICE
EPA Form 2220-1 (Rev. 4-77) PREVIOUS EDITION IS OBSOLETE
F:\U\FMeadows\TRD.Frm\WP 6.1
------- |