Integrated Iron and Steel Industry
Final Report
Volume III of III
Appendices
Contract No. 68-D7-0068
Work Assignment 2-13
LTV Steel Company
Indiana Harbor Works
East Chicago, Illinois
Prepared for:
Michael K. Ciolek
Emission Measurement Center
Emission, Monitoring, and Analysis Division
Office of Air Quality Planning and Standards
U.S. Environmental Protection Agency
Research Triangle Park, North Carolina 27711
August ,999 a
5 Region 5, Library
*•"""
77 West Jackson Boulevard, 12th Floor
Chicago, H 60604-3590
EASTERN RESEARCH GROUP, INC.
-------
Table of Contents
Appendix C Method 29, Analytical Data for Metals
Appendix D Gravimetric Analysis Data
Appendix E Field Data
E. 1 Method 23 and Method 29 Field Data Sheets
E.2 Meter Box Calibrations
E.3 Chain-of-Custody Sheets
E.4 Summary of Sampling Parameters
-------
Appendix C
Method 29
Analytical Data for Metals
cah/K.\7997\03\07-RPT\APX-CVR.WP6
-------
CASE NARRATIVE
Analysis of Samples for the Presence of Trace Metals
Method 29 April 1996 Rev.
Client: Eastern Research Group
TLI Project Number: 42298
Date: August 1, 1997
This report should only be reproduced in full.
Any reproduction of this report requires permission from
Triangle Laboratories, Inc.
Rev. 25-Sep-96
Triangle Laboratories, Inc.
801 Cap/to/a Drive P.O. Box 13485
Durham, NC 27713-4411 Research Triangle Park, NC 27709-3485
919-544-5729 Fax #919-544-5491
-------
Triangle Laboratories, Inc. August 1,1997
Case Narrative TLI Project #: 42298
Overview
Six train samples, two field blank train samples and a three reagent blanks were analyzed
for arsenic (As), beryllium (Be), cadmium (Cd), cobalt (Co), chromium (Cr), manganese
(Mn), nickel (Ni), lead (Pb), antimony (Sb), selenium (Se), and mercury (Hg). For all
analyses, the samples and associated QC samples were prepared and analyzed following
the guidelines of Method 29 April 1996 Rev. Results reported relate only to the items
tested.
OC Remarks
The release of this set of data by Triangle Laboratories, Inc. was authorized by the Quality
Control Chemist who has reviewed each sample data package individually following a
series of inspections/reviews. When applicable, general deviations from acceptable QC
requirements are identified below and comments are made on the effects of these
deviations upon the validity and reliability of the results. Specific QC issues associated
with this particular project are:
Sample Receipt:
The HNO3 rinses, back half impingers, and the Hg impingers for eleven train samples were
received without coolant on July 01,1997 under project # 42298 in good condition. The
0. IN HNO3 rinse samples (LTV-96 and LTV-87) were received without coolant on July 01,
1997 under project # 42298 in good condition and put on hold per the client's request The
filters and acetone probe rinses for the associated ten train samples were received without
coolant on July 14, 1997 under project # 42434 in good condition. All samples were
combined and processed under project # 42298. The data for all the samples were reported
under project # 42298. . - \ >>.''•"
/<" " ' ' ."'' ' '
Samples LTV-59, LTV-57, and LTV-87 were not listed on the client's chain-of-custody.
The sample labels were used to identify these samples. Sample LTV-59 was also identified
as Method 29, Inlet, RB2 on the sample bottle. Upon further discussion with the client, it
was noted that the ID for this sample should be Method 29, Inlet, RB3. The corrected ID
was used to identify this sample.
Sample Preparation:
Laboratory documentation of the sample preparation is included in the data package.
Instrumentation:
Arsenic (As), beryllium (Be), cadmium (Cd), cobalt (Co), chromium (Cr), manganese
(Mn), nickel (Ni), lead (Pb), antimony (Sb), and selenium (Se) concentrations were
determined by Inductively Coupled Plasma Emission Spectroscopy (ICP).
-------
Triangle Laboratories, Inc. August 1,1997
Case Narrative TLI Project*: 42298
Mercury (Hg) concentrations were determined by Cold Vapor Atomic Absorption
(CVAA).
The linear range for the instrument TJA 6IE Trace Analyzer was based on four standards
and a blank, which established a correlation coefficient value greater than or equal to
0.995. A calibration curve, based on a blank and one standard, is established for each
analytical run, followed by a check high standard and an initial calibration verification
(ICV). The check high standard does not deviate from the calibration curve by more than
5%. In addition, continuing calibration verifications (CCVs) are performed throughout
the analytical run.
A Reporting Detection Limit (RDL) is used instead of an Instrument Detection Limit
(IDL). The spectrometer and atomic absorption instruments can achieve low detection
limits between 0.2-8 ppb levels for many analytes. Triangle Labs is using RDL values of
1-10 times the DDL as detection limits for reporting purposes.
Data Review:
All analytes found in the method blank (MB) are detected at a level equal to or less than
the respective Reporting Detection Limits (RDLs).
A sampling date was not supplied by the client and the sampling to analysis holding times
cannot be determined. All samples were analyzed within 16 days of sample receipt at
Triangle Laboratories.
The laboratory control sample (42298 LCS1) for Hg demonstrated a percent recovery
slightly outside the QC criteria, but should not cause a bias towards the sample
concentrations. Please note that the associated laboratory control sample duplicate
(42298 LCS 1 D) demonstrate a percent recovery within QC criteria. All related calibration
samples (i.e. ICV, ICB, CCV, CCB etc.) were within the method criteria, which indicates
that the instrument was operating properly.
The serial dilution results for Cr for sample LTV-88 & 2 & LTV-02,101 FH demonstrated
a RPD slightly outside the QC control criteria of 10.0 percent, which does not indicate the
presence of a significant amount of interferents specific to this analyte in the native sample
matrix.
The recoveries for the post-digestion spike (PDS) are not reported for Cd, Mn, Ni, and Pb
for sample LTV-88 & 2 & LTV-02,101 FH. The spike concentrations added were
insignificant in comparison to the levels of these analytes present in the native sample.
The concentration for Pb for the post-digestion spike (PDS) was above the linear range of
the instrument and therefore, was not reported on the reporting forms.
-------
Triangle Laboratories, Inc. August 1,1997
Case Narrative TLI Project*: 42298
QC requirements:
The analytical duplicates for analytes analyzed by ICP cannot be considered valid
qualifiers if the concentrations of the analytes in the original and/or duplicate sample are
not at least ten times the respective RDLs. The RPDs for these analyses are indicated by
or "
-------
- y
TRIANGLE LABORATORIES, INC
UST OF CSTHRCATICNS AND ACCREDITATIONS
gflVIRCNMgMTAL
American Association for Laboratory Accreditation. Expires Jury 31, 1997. Certificate
Number 0226-01. Accreditation for tecnracaj competence in Environmental TastingXIndudfrig
Waste Water. Soi/Haz Waste, Pulp/Paper, and Air Matrices) Parameters are AOX/TQX.
Vdatiles. Pesticides. PCS's. SNA's, and Dtain/Furan. Metncd 1613 for Drinking Water.
State of Alabama, Department of Environmental Management. Expires December 31,
1997. Laboratory I.D. f 4C95Q. DIoxin in drinking water.
State of Alaska, Department of Environmental Conservation. Expires December 21,1997.
Certificate number OS-OQ397. Dfoxin in drinking water.
Stats of Arizona, Department of Hearth Services. Expires May 26. 1997. Certificate
*AZQ422. Drinking Water far Oioxin, Qtaxm in WW and S*H Waste.
Slats of Arkansas, Department of Pollution Control and Ecology. Expires February 18,
1998. Pulp/paper, soil, water, and Hazardous Waste for Dfaxin/Furan; AOXTPOX
Stats of California, Department of Heatin Services. Expires August 31. 1997. Certificate
*1922, Selected Metais in Waste Water; Vdatfles, Serrn-voiaffles, and Otaxm/furan in WW and
Sd/Haz Waste. Dtasn in drinking water. -
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Registration # PH-0117. Dfoxin in drinking water.
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Dtaxin in drinking water.
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DW. Drinking Water !O HRS^ 37424. Metaev Extractable Crganics (GC/MS).
(GC) and Voiatiles (GC'MS) in Environmental Samples. Enviionmenlal water 10 HRS*
!na
.Ba
tMaat,NC27713-4*n nmtmnH THang* Ptrit, JHC 277094485
-------
Hawaii Department of Heaft. Expires Marc: 1, 1998. Cicxin in drinking water. 'Accepted*
for regulatory purposes.
Idaho Department of Heart and Welfare. Expires November 30, 1997. DToxin in drinking
water.
State of Kansas, Depart*** of Hearth and Environment Expires January 31, 1998.
Environmental Analyses/Nan pofade Water and Sotid and Hazardous Waste. Method 1613
for drinking 'Mater. ID ^-Qinlong water and/or poflutfen ccntrd - E-215. Sdid or Hazardous
Waste-£-1209.
Commonwealth of K«andqr, Department for Environmental Protection. Expires
December 31,1997. IDaOQBL Oioxin in drinking -water.
Maryland Department of ftaaOn and Mental Hygiene. Expires September 3C, 1997.
Certification 2225. Driridag^eteray Method 1613A.
State of Michigan, DevJUUBM. of Public Heaflh. Expires March 31,1997. Drinking water by
Method 1613.
Mississippi State Dqmtaem of Hearth. No expiration date.. Oioxin in drinking water.
Montana Department of Heeft and Environmental Services. Expires December 31,1997.
DIoxn in drinking'
State of New Jersey, Deyjiuietu of Environmental Protection and Energy. Extended by
state. Temporary cenfficafe anal June 30, 1997 or sooner. ID #67851. SNAs and Voiatfles.
Dtoxin in drinking
State of New Mearico, Dmuuuieiit Oepartrnent Expires Juiy 31, 1997. Dioxin in
water.
New York State Departee* of Health. Expires June 30, 1997. 10 $11026. Environmental
Analyses of non-odaote Wata; Solid and Hazardous Waste. Method 1613 in OW.
State of North Carafea, Pqmaueiu. of Di»iiuiuiie»t Health and Natural Resources
Expires December 31,1997. Certificate f 37751. Otoon in Omikuicj water.
State of North Caranoi* Oepvtment of Etivu ui unent^ IfejiUiy and Natural Hesoui1 CB>S»
Division of CjiniiuiimaH ••iiijiiiniinr. Expires Oecember 31,1997. Certiffcate * 485.
Metais, pesticdes & PHH ani yuliitlJi.'v and vdatfles; TCLP.
North Dakota Stati QcpBtoent of iledlth ano> Consoiktated L4oui4tune-s» Expires
Oecsmber3l, 1997. Caftat* fi-076. ESecSv«Cctober4,1993. Ofooon in drinking water.
May 20.
-------
Oklahoma Department of &iviimuue»ul Quality. Expires October 31, 1997. Laboratory
£9612. Oioxin by 1613A, 3290 and 3280.
Stata of South Carolina, Department of Health and Environmental Control. Expires April
1, 1997. Certificate number 199040001 (drinking water). Expires August 31, 1997. Certificate
number #99040002 (other parameters). daxn/Rtrans, SNA, Volatfles, and PCSs/pesncoes
under Clean Water Act 13.7,3-TCOO for Drinking Water, and Organic extractables for Solid
and Hazardous Waste.
State of Tennessee. Derailment of Environment and Conservation. Expires February 5,
1999.10 #32992. Method 1613 Drinking water oniy.
LLS. Department of Agriculture Soil Permit Expires September 30, 2Q02. Permit No. S-
4958. Under the authority of the Federal Plant Pest Ac, permission is granted to receive
foreign sal samples for use in laboratory analysis.
U.S, Army Carps of Qiqinea-s. Expires November 30, 1997. Validated to perform methods
8280 & 3290 for Lcckbcume Landfifl Ste Investigation. Defense Distribution Depot Projects,
and assorted projecs for the USAGE North Pacific Division Laboratory.
EPA Region V. Expires November 14, 1999. Dwxin in drinking water.
SPA Region VB, for the Slate of Wyoming. Expires November 13, 1997. Dicxin in
drinking water.
Stata of Utah, Derailment of Health. Expires December 31, 1997. Certificate Number E-
166. Certification for the Mowing parameters: Sena-Voiatfles and Voiatfles under RCRA;
Volatfles under dean Water Act DknaVfurans by Method 3280; Drinking water for Dicxin by
Method 1613; MetaJs inducing Mercury and Vficrawave Digesticn.
Commonwealth of Virginia, Derailment of General Services, Oivtsicn of Consolidated
Laboratory Services. Expires June 30,1997. ID # 00341. Dicxin in drinking water.
Stata of Washington, Deponent of Ecology. Expires September 11, 1997. Lab
Accreditation Number C067. Scope of Accredfaticn appfies to water analyses for
Porycniorinated DBjenzD-p-claxiRs and PoiycWorinated Dajenzofurans, SNA Extr (Semivciat8e)
Organics and Purgeafate (Volafle) Organics.
Stata of Washtngton, Deuamiieni of Hearth. Expires April 30,1998. Dicxin in drinking water.
Lab I.0.129
Stata of West Virginia, Depaitiiiau of Health. Expires December 31, 1997. Certificate No.
9923(0). Cloon in anting water.
-------
State of Wisconsin, Depaaaeut at Nattrai Resources. Expires June 30.19S7. Laboratory
ID Numoer 999869530, CartScanan for ttie fancying categories of Orgamcs: Purgesbie,
Base/Neutral AcidL PC3i and Dfam Expires November 14, 1999. Laboratory (0
999865530. Clean in drintaog' '
Drug Enforcement Ageaqr ODEA). Expires November 30, 1997. Registration number
RTQ1195835. Corarcded ateiancs rBgisSaricn for schedules 1Z3,3N,4,5.
M.C. Department of Hun Resources. Expires October 31, 1997. Registration number
NC-?T 0000 0031. North Canina controied substances registration. Application submitted for
renewal.
Food 4 Drug Maamtatat (FDA) Registration. Expires Jury 1997. ID *s 001500 1053481.
Annual registration of drug estabishrnent. Annual registranon of drug estabiisftrnerrL
Ofnicai Laboratoy (mpravement Amendments (CUA) Registration. Expires .Viay 30. 1999.
ID * 3400705123. Depateaa'it of Health & Human Services. Heaim Care Financing
Administration,
U.S. EPA Large Quamfey H^»-"'»im Waste Generator. No expiration date. EPA ID
#NCC9821 56379. Pamt nftates tftatlhe laboratcny is a large generator of hazardous waste.
Nortn Caroiina RaftiJiriiie Haieriais License. Expnes April 30 1998. License No. 032-
0954-1 . Licsnse- auttiuius fte Jcasa? to recerve, acquire, own, possess* transfer, import and
use SUCfl i
North Carolina General license tar Radiation Protection. No. aapiiatluii date. License No.
032-375-OG. The geneal fcense appies only to radioactive material contained in devices
which have been manufaeaged and labeled in accordance with specific requirements.
— 8
-------
ABBREVIATIONS
BH « Back Half
CCB = Continuing Calibration Blank
CCV = Continuing Calibration Verification
CHECK HS = Check High. Standani
D = OLT = Analytical Duplicate (Prepared Duplicate)
DA = Duplicate Analysis
FH = Front Half
FV s Hnai Digestate Volume
ICB «Itrinal Calibration Blank
ICV = Ininal Calibration Verification
ICS AB = Interference Check Solution (Solution AB)
I = Tnirial
F = Final
Solution AB contains common Jnraiiaeais in addition co the analyte of interest.
DDL = Instrument Detection Limit
L = Serial Dilution
LCS = Laboratory Control Spike Sample
MB = Method Blank
MPV = Mercury Preparation Volume
MS = Pre-digestion Spike
MSD = Pre-digestion Spike Duplicate ^
N/A = Noc Applicable
N/Av = Not Available
N/V = Not Valid
PDS = Post-digestion Spike
%REC = Percent Recovery
RDL = Reporting Detection TJmif
RPD = Relative Percent Difference
T = Analytical Triplicate (Prepared TnpBcate; for Hg analysis by Method 7471 only)
TV = Total Sample Volume
< = Analyte concsnrranon in the .sample is less than the respective RDL
-------
STANDARD CONCENTRATIONS
for the TJA 61E TRACE ANALYZER
Anaivte I Units ! ffignStd ' ICV/CCV I ICSAB
RDL I Wavelength
JEg " £' rob? i
rob I 1000
500 - I 1
^Ji>;~5SO--
:;
Note: Use this reference page to review the raw data from the TJA 6 IE Trace Analyzer.
This page includes tbc standard concentrations for the check high standard, iniriai calibradon
verification (ICV), continuing caiifaranon verincarion (CCV), and the interference check solution
(ICSAB). In addidon tbe reporting detection limit (RDL) and wavelength are reported for each
analyte.
Revision Date: 15-Jui-96
- 10
-------
CALCULATIONS FOR AIR SAMPLES
RESULTS FOR TRACE METALS (except mercury):
RESULT in ng (Front Half) = ag/L * FV (mL) * DF
1000 mL/L
RESULT in |ig (Back Half & Impingers) = p.g/L * TV CmU) * FV (mL) * DF
mL used* 1000 mL/L
FV = final volume in mL
TV = total volume in mL
DF = Dilution Factor
The RESULTS for combined Front Half & Back Half samples use the same calculation as the
Back Half & impinger samples.
RESULTS FOR MERCURY (He);
RESULT in jig (Front Half) = |ig/L * (mL FV/mL aliquot) * MPV * DF
RESULT in |ig (Back Half & Impingers) = (ig/L * (mL TV/mL aliquot) * MPV * DF
MPV = mercury preparation volume = 0.1 L
%REC (Percent Recovery) for MS/MSP He spikes:
%REC = spike sample results - original sample results * 100
true spike sample results
NOTE: Original sample results less than the RDL are not used in calulations.
%REC rPercent Recovery) for PDS:
%REC = Spike sample u.g/L cone. - original sample |ig/L eonc. * 100
spike cone. (u.g/L)
%REC (Percent Recovery) for LCS/LCSD:
%REC = Spike sample u.g/L cone. * 100
spike cone.
RPD = I Result 2 - Result 1 I * 100
(Result 2 + Result l)/2 Rev. 2-Oct-96
11
-------
Client: Eastern Research Group
Project Number: 42298
Sample Report
Client Sample ID:
TLI Sample H>
Date Received:
Date Prepared:
Date Analyzed'
Matrix:
LTV-88 & 2 & LTV-02.101 FH
174-97-11.1 & 173-60-1 A.10FH
Julv 01 & 14. 1997
July 18-25. 1997
Julv 28. 1997
Air
Aoalvte
As
Be
Cd
Co
Cr
Mn
Ni
Pb
Sb
Se
Concx.
fcoAi
46.257
0.259
726.988
-7.271
216.987
535.365
817.800
30775.289
60.445
169.688
anL.. .:...
TotaJVoL
N/A
N/A
N/A
N/A
N/A
N/A
N/A
N/A
N/A
N/A
•..:..-;frt.
Used
N/A
N/A
N/A
N/A
N/A
N/A
N/A
N/A
N/A
N/A
mLr^
final Vfct:
100
100
100
100
100
100
100
100
100
100
• ' LnfUttQn
• factor
1
1
1
1
1
1
1
5
1
1
• Total UQ
Resutt
4.63
< 0.100
72.7
< 0.100
21.7
53.5
81.8
15400
6.04
17.0
Triangle Laboratories, Inc.
801 Capitola Drive * Durham, North Carolina 27713
Tele: (919) 544-5729 * Fax: (919) 544-5491
Printed: 30-M-97 at 09:34 AM
12
-------
Client: Eastern Research Group
Project Number: 42298
Sample Report
Client Sample ID:
TLI Sample ID:
Date Received:
Date Prepared:
Date Analyzed:
Matrix:
LTV-88&2<V-02.101
FHL
174-97-11.1 & 173-60-1 A.10FHL
Julv 01 & 14. 1997
Julv 18-25. 1997
Julv 28. 1997
Air
Analyte
As
Be
Cd
Co
Cr
Mn
Ni
Pb
Sb
Se
Cona
fcoto
7.927
0.136
153.150
-1.256
48.990
108.372
172.627
6354.457
14.467
37.387
!• •«&•-.
: Total Voi;
N/A
N/A
N/A
N/A
N/A
N/A
N/A
N/A
N/A
N/A
:----:-*rtL:. ,
•' : Useef
N/A
N/A
N/A
N/A
N/A
N/A
N/A
N/A
N/A
N/A
-• -fBt.
RreaVoL
100
100
100
100
100
100
100
100
100
100
:OP»n
;f3lebr
5
5
5
5
5
5
5
25
5
5
Totefug
Result
3.96
< 0.500
76.6
< 0.500
24.5
54.2
86.3
15900
7.23
18.7
Triangle Laboratories, Inc.
801 Capitola Drive * Durham, North Carolina 27713
Tele: (919) 544-5729 * Fax: (919) 544-5491
Printed: 30-JuI-97 at 09:34 AM
13
-------
Client: Eastern Research Group
Project Number: 42298
Sample Report
Client Sample ID-
TLI Sample ID:
Date Received:
Date Prepared:
Date Analvzed:
Matrix:
LTV-03 BH
173-60-1B BH
Julv 01 & 14. 1997
July 18-25, 1997
Julv 28. 1997
Air
Artafyte
As
Be
Cd
Co
Cr
Mn
Ni
Pb
Sb
Se
: Cone,
&t*U
0.216
0.205
5.910
-0.565
25.395
101.394
38.396
71.842
2.266
168.572
roL . -
! •= TotalVdi:
670
670
670
670
670
670
670
670
670
670
. • JPt". . .
••'Used
570
570
570
570
570
570
570
570
570
570
:---.:'. acr.""
RrcidVbi; ;
100
100
100
100
100
100
100
100
100
100
-: ixpsubor* .
-OFkrtor
1
1
1
1
1
1
1
1
1
1
Totefug
Result
< 0.588
< 0.118
0.695
< 0.118
2.98
11.9
4.51
8.44
< 0.470
19.8
Triangle Laboratories, Inc.
801 Capitola Drive * Durham, North Carolina 27713
Tele: (919) 544-5729 * Fax: (919) 544-5491
Printed: 30-M-97 at 09:34 AM
14
-------
Client: Eastern Research Group
Project Number: 42298
Sample Report
Client Sample ID:
TLI Sample ID:
Date Received"
Date Prepared:
Date Analyzed:
Matrix:
LTV-03 BH L
173-60-1B BH L
Julv 01 & 14. 1997
Julv 18-25. 1997
Julv 28. 1997
Air
Analyte
As
Be
Cd
Co
Cr
Mn
Ni
Pb
Sb
Se
Cona
fco«
-1.318
0.069
1.119
0.182
5.556
19.982
7.849
18.600
0.522
36.695
• jflL-"'
Total Vol.
670
670
670
670
670
670
670
670
670
670
< *C.r">
;=.:--tfee£-v
570
570
570
570
570
570
570
570
570
570
"•- #L. -•:
finsWoi.
100
100
100
100
100
100
100
100
100
100
: : HwfiQO I
; 'factor^
5
5
5
5
5
5
5
5
5
5
:: Tofcftig
Result
< 2.94
< 0.588
0.658
< 0.588
3.27
11.7
4.61
10.9
< 2.35
21.6
Triangle Laboratories, Inc.
801 Capitola Dnve * Durham, North Carolina 27713
Tele: (919) 544-5729 * Fax: (919) 544-5491
Printed: 30-M-97 at 09:34 AM
15
-------
Client: Eastern Research Group
Project Number: 42298
Sample Report
Client Sample ED:
TLI Sample ID-
Date Received:
Date Prepared:
Date Analyzed:
Matrix:
LTV-89 & 3 & LTV-08 FH
174-97-13.4 & 173-60-2A FH
Julv 01 & 14. 1997
Julv 18-25. 1997
Julv 28. 1997
Air
Analvte
As
Be
Cd
Co
Cr
Mn
Ni
Pb
Sb
Se
MJnC. ..;.;
43272
0.250
674.566
0.855
171.701
561.112
1166.381
15047.530
58.077
186.641
- rrt
VOL.
r Total VbL:-
N/A
N/A
N/A
N/A
N/A
N/A
N/A
N/A
N/A
N/A
•'i&d-' '•
N/A
N/A
N/A
N/A
N/A
N/A
N/A
N/A
N/A
N/A
_l :
': • WL.
100
100
100
100
100
100
100
100
100
100
•vJ5S^
1
1
1
1
1
1
1
10
1
1
; Result
4.33
< 0.100
67.5
< 0.100
17.2
56.1
117
15000
5.81
18.7
Triangle Laboratories. Inc.
801 Capitola Drive " Durham, North Carolina 27713
Tele: (919) 544-5729 * Fax: (919) 544-5491
Printed: 30-M-97 at 09:34 AM
16
-------
Client: Eastern Research Group
Project Number: 42298
Sample Report
Client Sample ID:
TLI Sample ID-
Date Received:
Date Prepared:
Date Analyzed:
Matrix:
LTV-89 & 3 & LTV-08
FHDA
174-97-13.4 & 173-60-2A FH DA
Julv 01 & 14. 1997
Julv 18-25. 1997
Julv 28. 1997
Air
Analyte ;
As
Be
Cd
Co
Cr
Mn
Ni
Pb
Sb
Se
Cone.
tarti
42.792
0.204
669.962
1.169
170.696
559.259
1160.938
14956.682
63.087
187.574
.. iflfc '
Tdfeftfet
N/A
N/A
N/A
N/A
N/A
N/A
N/A
N/A
N/A
N/A
-roL I-
US6d::
N/A
N/A
N/A
N/A
N/A
N/A
N/A
N/A
N/A
N/A
fit
Final Vol.
100
100
100
100
100
100
100
100
100
100
j £J&rtfc>r>
Factor
1
1
1
1
1
1
1
10
1
1
• Total- ug
Result
4.28
< 0.100
67.0
0.117
17.1
55.9
116
15000
6.31
18.8
Triangle Laboratories, Inc.
801 Capitola Dnve * Durham, North Carolina 27713
Tele: (919) 544-5729 * Fax: (919) 544-5491
Printed: 30-M-97 at 09:34 AM
17
-------
SE'3-17-97 WED 05 = 53 PM TRIANGLE LABS
FAX NO, 919+544+5491
P. 03
Client: Eastern Research Group
Project Number; 42298
Sample Report
Client Sample ID:
11! Samnle ID:
Datf Received:
f>ate Preoared:
Jafc Anilvred'
v^atrix:
LTV-Oy BH
173-6G-2B BH
Julv 01 & 14. 19Q7
Julv 18-25. 1997
lulv 2*. 1997
Air
;- •A'aaMs.-.':"':;:
As
Be
Cd
Co
Cr
Mn
Ni
Pb
Sb
Se
ViC.gOflC;'1;"}
V-.fctefe^
-2.8O1
0.065
-0.318
-1.593
12.890
205645
4,377
9.815
2.228
139.641
:^?1&^
>i^H-siab>;
660
660
660
660
660
660
660
660
660
1 660
!:;f|.:^TT|iij;;-;;;
xx''~:;MS8$:yv£
560
560
560
560
560
560
560
560
560
560
ti-.*'W:'£ti
:;'&&8ti&$?:
100
100
100
100
100
100
100
100
100
100
;"*v!5iteiSDfi&"j
'f£z&&&£%
1
1
1
1
1
1
1
i
i
1
-
^^T^^'uo ''•"., :-';
v^il^iftvv-:
< 0.589
< 0.118
< 0.118
< 0.118
1.5?
242
0.516
1.16
< 0.471
16.5
i
rcngle I-aboratories, Inc.
C1 Capitola Drive * Durham. Nonn Carolina 27713
Jtlc {yi9> 544-5729 ' TAX. (9l'J» 544-5491
Printed: 30-Jul-97 at 09:34 AM
18
-------
Client: Eastern Research Group
Project Number: 42298
Sample Report
Client Sample ID-
TLI Samole ID-
Date Received:
Date Prepared:
Date Analyzed:
Matrix:
LTV-09BHDA
173-60-2BBHDA
Julv 01 & 14. 1997
July 18-25, 1997
Julv 28. 1997
Air
Analyte
As
Be
Cd
Co
Cr
Mn
Ni
Pb
Sb
Se
Cone.
fctfD .
-4.576
0.081
-0.343
-1.807
12.366
206.673
4.301
9.255
1.696
134.400
vL
TotalVolv
660
660
660
660
660
660
660
660
660
660
nt- •-
Used;:
560
560
560
560
560
560
560
560
560
560
fit
RnalV&
100
100
100
100
100
100
100
100
100
100
;Diution
'- Factor
1
1
1
1
1
1
1
1
1
1
Totefiig
Result
< 0.589
< 0.118
< 0.118
< 0.118
1.46
24.4
0.507
1.09
< 0.471
15.8
Triangle Laboratories. Inc.
801 Capitola Drive * Durham, North Carolina 27713
Tele: (919) 544-5729 * Fax: (919) 544-5491
Printed: 30-Jul-97 at 09:34 AM
19
-------
Client: Eastern Research Group
Project Number: 42298
Sample Report
Client Sample ED:
TLI Sample ED:
Date Received:
Date Prepared:
Date Analyzed:
Matrix:
LTV-90 & 4 & LTV-14 FH
174-97-15.6 & 173-60-3A FH
July 01 & 14, 1997
July 18-25. 1997
July 28, 1997
Air
Anaivie
As
Be
Cd
Co
Cr
Mn
Ni
Pb
Sb
Se
., .Cof»; .
-" «T
38.957
0.213
726.763
-7.951
174.490
1147.143
664.175
16315.991
63.037
168.328
: ' raL
1 TbtetVsL
N/A
N/A
N/A
N/A
N/A
N/A
N/A
N/A
N/A
N/A
rrL
Userf
N/A
N/A
N/A
N/A
N/A
N/A
N/A
N/A
N/A
N/A
rnL;:::::,:;
RnafV&
100
100
100
100
100
100
100
100
100
100
:: -Dfl&fcar: .:
:"';!3EK*#i:v:'':
1
1
1
1
1
1
1
10
1
1
, lotakug 1;
•' -'Resafr :'|:
3.90
< 0.100
72.7
< 0.100
17.4
115
66.4
16300
6.30
16.8
Triangle Laboratories, Inc.
801 Capitola Drive * Durham, North Carolina 27713
Tele: (919) 544-5729 * Fax: (919) 544-5491
Printed: Ol-Aug-97 at 12:52 PM
n
0
-------
Client: Eastern Research Group
Project Number: 42298
Sample Report
Client Sample ID:
TLI Sample ID-
Date Received:
Date Prepared:
Date Analyzed:
Matrix:
LTV- 15 BH
173-60-3B BH
Julv 01 & 14. 1997
Julv 18-25. 1997
Julv 28. 1997
Air
Analyte
As
Be
Cd
Co
Cr
Mn
Ni
Pb
Sb
Se
Cone.
-3.089
0.201
-0.030
-0.935
16.983
2681.926
4.349
16.677
4.028
161.227
'- ••. ,1 - --
. nm.. tf.f
! TbialVbif
690
690
690
690
690
690
690
690
690
690
•:.- : -. -." fn(»»;:".:--- .---:-•-
• ' •-' fcfeed::. :":-:
590
590
590
590
590
590
590
590
590
590
,, :,v:)Tt.
Final Vol;
100
100
100
100
100
100
100
100
100
100
- • rvtt. ji—_
UMUUQf}
: Factor
1
1
1
1
1
1
1
1
1
1
lotatuq
Result
< 0.585
< 0.117
< 0.117
< 0.117
1.99
314
0.509
1.95
0.471
18.9
Triangle Laboratories, Inc.
801 Capitola Dnve * Durham, North Carolina 27713
Tele: (919) 544-5729 * Fax: (919) 544-5491
Printed: 30-Jul-97 at 09:34 AM
21
-------
Client: Eastern Research Group
Project Number: 42298
Sample Report
Client Sample ID'
TLI Sample ID:
Date Received:
Date Prepared:
Date Analvzed:
Matrix:
LTV-39 & 8 & LTV-38 FH
174-97-18.8 & 173-60-4A FH
Julv 01 & 14. 1997
Julv 18-25, 1997
Julv 28. 1997
Air
\;
Analyte
As
Be
Cd
Co
Cr
Mn
Ni
Pb
Sb
Se
Cona
foo/U
5.776
0.056
-5.083
-13.712
115.477
140.317
490.045
270.535
62.157
58.509
" Wt."-;"
•! TbtalVdv
N/A
N/A
N/A
N/A
N/A
N/A
N/A
N/A
N/A
N/A
•J: -:nt-.V.
• •• " Us***:'
N/A
N/A
N/A
N/A
N/A
N/A
N/A
N/A
N/A
N/A
••„• .--wt.-. -.
RnalVot;
100
100
100
100
100
100
100
100
100
100
' 'O&itor*
: Factor
1
1
1
1
1
1
1
1
1
1
Total ug
ftesult
0.578
< 0.100
< 0.100
< 0.100
11.5
14.0
49.0
27.1
6.22
5.85
Triangle Laboratories, Inc.
801 Capitola Drive * Durham, North Carolina 27713
Tele: (919) 544-5729 * Fax: (919) 544-5491
Printed: 30-M-97 at 09:34 AM
22
-------
Client: Eastern Research Group
Project Number: 42298
Sample Report
yv
Client Sample ID:
TLI Sample ID-
Date Received:
Date Prepared:
Date Analyzed:
Matrix:
LTV-40,38 BH
173-60-4B.4A BH
Julv 01 & 14. 1997
Julv 18-25. 1997
Julv 28. 1997
Air
Analvte- ''•
As
Be
Cd
Co
Cr
Mn
Ni
Pb
Sb
Se
VConc.
: {uoflJ
-3.540
0.050
0.261
-0.905
12.973
157.365
4.587
39.868
-1.279
12.049
:;:- -V-1BL--
i&feivbi
300
300
300
300
300
300
300
300
300
300
ITL
Used
300
300
300
300
300
300
300
300
300
300
Hi
KnaJVof.
100
100
100
100
100
100
100
100
100
100
Diufcxr
Factor
1
1
1
1
1
1
1
1
1
1
:.: '*$}*$&"• " .;
Result
< 0.500
< 0.100
< 0.100
< 0.100
1.30
15.7
0.459
3.99
< 0.400
1.20
Triangle Laboratories, Inc.
801 Capitola Drive * Durham, North Carolina 27713
Tele: (919) 544-5729 * Fax: (919) 544-5491
Printed: Ol-Aug-97 at 12:52 PM
23
-------
Client: Eastern Research Group
Project Number: 42298
Sample Report
Client Sample ID:
TLI Sample ID:
Date Received:
Date Preoared:
Date Analyzed:
Matrix:
LTV-52& 10<V-51FH
174-97-19.9 & 173-60-5AFH
Julv 01 & 14. 1997
Julv 18-25. 1997
Julv 28. 1997
Air
Arialvte
As
Be
Cd
Co
Cr
Mn
Ni
Pb
Sb
Se
footo
3.659
-0.009
-7.418
-14.652
105.582
55.734
248.809
92.009
60.668
52.007
I iiiaim--
N/A
N/A
N/A
N/A
N/A
N/A
N/A
N/A
N/A
N/A
• &5ed.:.V'
N/A
N/A
N/A
N/A
N/A
N/A
N/A
N/A
N/A
N/A
Rh^Vof.:
100
100
100
100
100
100
100
100
100
100
factor
1
1
1
1
1
1
1
1
1
1
Total UQ
: Result
< 0.500
< 0.100
< 0.100
< 0.100
10.6
5.57
24.9
9.20
6.07
520
Triangle Laboratories, Inc.
801 Capitola Drive * Durham, North Carolina 27713
Tele: (919) 544-5729 * Fax: (919) 544-5491
Printed: 30-M-97 at 09:34 AM
24
-------
Client: Eastern Research Group
Project Number: 42298
Sample Report
Client Sample ID:
TLI Sample ID:
Date Received:
Date Prepared:
Date Analvzed:
Matrix:
LTV-53,51 BH
173-60-5B.5A BH
Julv 01 & 14. 1997
Julv 18-25. 1997
Julv 28. 1997
Air
AnaMe- ;
As
Be
Cd
Co
Cr
Mn
Ni
Pb
Sb
Se
c vGona
*'i'!WU
-4.576
0.129
0.373
-1.180
12.646
1240.667
3.475
129.916
-0.536
10.086
i mL
! ToiafVd,
300
300
300
300
300
300
300
300
300
300
ffL
Used
300
300
300
300
300
300
300
300
300
300
Bt
RnaJVoi
100
100
100
100
100
100
100
100
100
100
D&d&EK
JEa£*bf;:k:::
1
1
1
1
1
1
1
1
1
1
-------
Client: Eastern Research Group
Project Number: 42298
n
Sample Report
Client Sample ID:
TLI Samole ID:
Date Received'
Date Prepared:
Date Analyzed:
Matrix:
LTV-58 FH
173-60-6 A FH
Julv 01 & 14 1997
Julv 18-25. 1997
Julv 28. 1997
Air
Analyte
As
Be
Cd
Co
Cr
Mn
Ni
Pb
Sb
Se
Cone.
&Q/U
-1.483
0.006
-0.530
-1.436
12.073
15.694
6.064
5.342
3.834
3.383
i • mt.
TotafVol
N/A
N/A
N/A
N/A
N/A
N/A
N/A
N/A
N/A
N/A
fl&
Used
N/A
N/A
N/A
N/A
N/A
N/A
N/A
N/A
N/A
N/A
mL
RnalVoi.
100
100
100
100
100
100
100
100
100
100
Slu6or»:
Sibctor
1
1
1
1
1
1
1
1
1
1
v •:. WtlQ .
lesutt
< 0.500
< 0.100
< 0.100
< 0.100
1.21
1.57
0.606
0.534
< 0.400
0.338
Triangle Laboratories, Inc.
801 Capitola Drive * Durham, North Carolina 27713
Tele: (919) 544-5729 * Fax: (919) 544-5491
Printed: 30-M-97 at 09:34 AM
26
-------
Client: Eastern Research Group
Project Number: 42298
Sample Report ;.-\
Client Sample ID:
TLI Sample ID-
Date Received'
Date Prepared:
Date Analyzed'
Matrix:
LTV-58,60 BH
173-60-6A.6C BH
Julv 01 & 14. 1997
Julv 18-25. 1997
Julv 28. 1997
Air
Anatvte
As
Be
Cd
Co
Cr
Mn
Ni
Pb
Sb
Se
Conc^
foafcfc -
-3.656
0.169
-0.289
-0.594
8.229
11.139
2.188
4.697
2.279
2.176
. . mL
TotalVol
150
150
150
150
150
150
150
150
150
150
,-jnL :=....
:Clsed
150
150
150
150
150
150
150
150
150
150
Rfc ......
RnalVoi:
100
100
100
100
100
100
100
100
100
100
Diuton
Saetor
1
1
1
1
1
1
1
1
1
1
Total us
: Result
< 0.500
< 0.100
< 0.100
< 0.100
0.823
1.11
< 0.300
0.470
< 0.400
< 0.300
Triangle Laboratories, Inc.
801 Capitola Drive * Durham, North Carolina 27713
Tele: (919) 544-5729 * Fax: (919) 544-5491
Printed: 30-M-97 at 09:34 AM
27
-------
Client: Eastern Research Group
Project Number: 42298
Sample Report
Client Sample ID:
TLI Sample ID-
Date Received'
Date Prepared:
Date Analyzed'
Matrix:
LTV-57 BH
173W-7 BH
Julv 01 & 14. 1997
Julv 18-25, 1997
Julv 28. 1997
Air
Analyte
As
Be
Cd
Co
Cr
Mn
Ni
Pb
Sb
Se
Cona
{vote
-6.245
0.108
-0.304
-0.912
9.524
35.882
4.083
6.893
-1.340
-1.281
— .mL.
i-:TeftdVofc
200
200
200
200
200
200
200
200
200
200
. • mL..... ••
Used
200
200
200
200
200
200
200
200
200
200
..... ..rot
Final Vol.
100
100
100
100
100
100
100
100
100
100
: Oiufior*
Factor
1
1
1
1
1
1
1
1
1
1
Total ug
Result
< 0.500
< 0.100
< 0.100
< 0.100
0.952
3.59
0.408
0.689
< 0.400
< 0.300
Triangle Laboratories, Inc.
801 Capitola Drive * Durham, North Carolina 27713
Tele: (919) 544-5729 * Fax: (919) 544-5491
Printed: 30-M-97 at 09:34 AM
28
-------
Client: Eastern Research Group
Project Number: 42298
Sample Report
Client Sample ED:
TLI Sample ID-
Date Received:
Date Prepared:
Date Analvzed:
Matrix:
LTV-46 & 9 & LTV-45 FH
174-97-20.10 & 173-60- 11A FH
Julv 01 & 14. 1997
July 18-25. 1997
Julv 28. 1997
Air
Analyte
As
Be
Cd
Co
Cr
Mn
Ni
Pb
Sb
Se
Cone.
&Krt.>
5.039
0.152
-9.533
-18.187
112.023
38.534
233.999
18.771
66.545
60.488
• .rut.
TdtalVd.
N/A
N/A
N/A
N/A
N/A
N/A
N/A
N/A
N/A
N/A
:-:':-pa>x'.' |fq« '.
SSipysed': '
N/A
N/A
N/A
N/A
N/A
N/A
N/A
N/A
N/A
N/A
fit
ErtfrfVof.
100
100
100
100
100
100
100
100
100
100
;ESufe>r*
Factor
1
1
1
1
1
1
1
1
1
1
Totafw
Result
0.504
< 0.100
< 0.100
< 0.100
11.2
3.85
23.4
1.88
6.65
6.05
Triangle Laboratories, Inc.
801 Capitola Drive * Durham, North Carolina 27713
Tele: (919) 544-5729 * Fax: (919) 544-5491
Printed: SO-Jul-97 at 09:34 AM
29
-------
Client: Eastern Research Group
Project Number: 42298
Sample Report
Client Sample ID:
TLI Sample ID:
Date Received:
Date Prepared:
Date Analvzed:
Matrix:
LTV-45,47 BH
173-60-11A.11BBH
Julv 01 & 14. 1997
July 18-25, 1997
Julv 28. 1997
Air
Analyte
As
Be
Cd
Co
Cr
Mn
Ni
Pb
Sb
Se
Co«x
ta*i'
-3.108
0.097
-0.165
-0.993
5.012
29.921
1.815
8.588
7.076
-0.628
; •• -;"f*fc
TofaiVoli
150
150
150
150
150
150
150
150
150
150
- i&L ' -
•<• a&d
150
150
150
150
150
150
150
150
150
150
' "WL :
Final Vol.
100
100
100
100
100
100
100
100
100
100
D&tiDft
Factor
1
1
1
1
1
1
1
1
1
1
Total y<3
Result
< 0.500
< 0.100
< 0.100
< 0.100
0.501
2.99
< 0.300
0.859
0.708
< 0.300
Triangle Laboratories, Inc.
801 Capitola Drive * Durham, North Carolina 27713
Tele: (919) 544-5729 * Fax: (919) 544-5491
Printed: 30-Jul-97 at 09:34 AM
30
-------
Client: Eastern Research Group
Project Number: 42298
Sample Report
Client Sample ED:
TLI Sample ID-
Date Received'
Date Prepared:
Date Analyzed:
Matrix:
LTV-91,99 & 5,12 & LTV-20 FH
174-97-1117.2.3 & 173-6Q-12AFH
Julv 01 & 14. 1997
Julv 18-25. 1997
Julv 28. 1997
Air
Aralyt& ;
As
Be
Cd
Co
Cr
Mn
Ni
Pb
Sb
Se
ConC.
: fcoto
141.540
-1.343
861.003
-0.511
841.898
13334.219
1193.349
19317.717
124.741
347.275
^4 aL
-ToteiVol
N/A
N/A
N/A
N/A
N/A
N/A
N/A
N/A
N/A
N/A
tit
Used
N/A
N/A
N/A
N/A
N/A
N/A
N/A
N/A
N/A
N/A
»t.
Final Vol.
100
100
100
100
100
100
100
100
100
100
D&rttor*
Factor
1
1
1
1
1
1
1
10
1
1
:/; totef yQ:
• ::Re!ailt
14.2
< 0.100
86.1
< 0.100
84.2
1330
119
19300
12.50
34.7
Triangle Laboratories, Inc.
801 Capitola Drive * Durham, North Carolina 27713
Tele: (919) 544-5729 * Fax: (919) 544-5491
Printed: Ol-Aug-97 at 01:01 PM
31
-------
SE-17-97 HED 04:3! PN TRIANGLE LABS
FAX NO, 919+54415491
P. 02
Client: Eastern Research Group
Project Number: 42298
Sample Report
riknt Sample ID:
n.l Sanrole ED:
")iitii Received:
>ate Prepared:
~>atc Analyzed'
vlatrix.
LTV-21 1311
173-60-12B BH
Julv 01 & 14. 1007
July 18-2?, 1997
Julv 28. 1997
Air
• ] Artelyte:' -,^:
As
Be
Cd
Co
Cr
Mn
Ni
PD
So _,
Se
J^vObhc.'1,'^
•••:••«$&&>•;>:
-1.114
0.017
7.374
0.557
58.352
437.650
40.027
808.638
0.113
126.506
V':^«^;>
^iwBM.-«
610
610
610
610
610
610
610
610
610
610
;':'S :&£••'*«••"
^i-:^4'^i
510
510
510
510
510
510
510
510
510
510
v:;fiba$$6&'£
100
100
100
100
100
100
100
100
100
100
^'^''jl^ailpfi1".;.
£::=:&&£(
1
i
1
i
i
i
i
1
1
1
•^BteftW-X>
^t:-$y«$r-:-! •-
< 0.598
< 0120
0.882
< 0.120
7.04
523
4.79
96.7
< 0.478
15.1
1
Triangle Laboratories, inc.
JO" Capitola Drive * Durham, North Carolina 27713
Icic: (919) 544-5729 * Fax: (9)9) 544-5491
Pncicd: 30-M-97 at 10:21 AM
32
-------
Client: Eastern Research Group
Project Number: 42298
Sample Report
Client Samole ID:
TLI Samole ID:
Date Received:
Date Prepared:
Date Analvzed:
Matrix:
LTV-92 & 6 & LTV-26 FH
174-97-14.5 & 173-60-13AFH
Julv 01 & 14. 1997
Julv 18-25. 1997
Julv 28. 1997
Air
Analvte
As
Be
Cd
Co
Cr
Mn
Ni
Pb
Sb
Se
Cona
fodU
184.349
-2.734
808.306
13.844
1009.181
18018.865
828.507
18498.926
99.302
405.634
i JBt'-V-"
Total %>r
N/A
N/A
N/A
N/A
N/A
N/A
N/A
N/A
N/A
N/A
. Mrrk.,:,i
:na*f.
-------
Client: Eastern Research Group
Project Number: 42298
Sample Report
Client Sample ID:
TLI Samole ID:
Date Received:
Date Prepared:
Date Analyzed:
Matrix:
LTV-27 BH
173-60-13B BH
Julv 01 & 14. 1997
Julv 18-25, 1997
Julv 28. 1997
Air
Aralyte
As
Be
Cd
Co
Cr
Mn
Ni
Pb
Sb
Se
Cone.
tarti
-2.825
0.055
-0.327
-1.497
12.701
52.151
8.878
10.712
-2.560
161.373
I' OIL ':•
i: .TotetVbte •
440
440
440
440
440
440
440
440
440
440
'•"Vrat'^X
: Used
340
340
340
340
340
340
340
340
340
340
•::'Hi;:.nC
100
100
100
100
100
100
100
100
100
100
Diuttor*
Factor
1
1
1
1
1
1
1
1
1
1
: Tctetfu<3
Result
< 0.647
< 0.129
< 0.129
< 0.129
1.64
6.75
1.15
1.39
< 0.518
20.9
Triangle Laboratories, Inc.
801 Capitola Drive * Durham, North Carolina 27713
Tele: (919) 544-5729 * Fax: (919) 544-5491
Printed: 30-M-97 at 10:21 AM
34
-------
Client: Eastern Research Group
Project Number: 42298
Sample Report
i- - •
Client Sample ID:
TLI Sample ID:
Date Received:
Date Prepared:
Date Analvzed:
Matrix:
LTV-93 & 7 & LTV-32 FH
174-97-16.7 & 173-60-14A FH
Julv 01 & 14. 1997
Julv 18-25. 1997
Julv 28. 1997
Air
Analvte
As
Be
Cd
Co
Cr
Mn
Ni
Pb
Sb
Se
Cone.
tarti-
200.979
-2.385
848.065
18.657
998.006
18995.707
869.776
19072.715
90.560
322.289
. ! mt .
!' TotaiVol
N/A
N/A
N/A
N/A
N/A
N/A
N/A
N/A
N/A
N/A
ni.. i.
-•• : Used
N/A
N/A
N/A
N/A
N/A
N/A
N/A
N/A
N/A
N/A
: :OB*. =
.'•"RttWofc
100
100
100
100
100
100
100
100
100
100
: fg^
1
1
1
1
1
1
1
10
1
1
;: ;Totai:u<3
: Result
20.1
< 0.100
84.8
1.87
99.8
1900
87.0
19100
9.06
32.2
Triangle Laboratories, Inc.
801 Capitola Drive * Durham, North Carolina 27713
Tele: (919) 544-5729 * Fax: (919) 544-5491
Printed: 30-M-97 at 10:21 AM
35
-------
Client: Eastern Research Group
Project Number: 42298
Sample Report
Client Sample ID:
TLI Sample ID:
Date Received:
Date Prepared:
Date Analvzed:
Matrix:
LTV-33 BH
1 73-60- 14B BH
Julv 01 & 14. 1997
Julv 18-25, 1997
Julv 28. 1997
Air
Analvte :
As
Be
Cd
Co
Cr
Mn
Ni
Pb
Sb
Se
Cone.
: to*)-
-4.527
0.074
-0.411
-1.021
15.393
97.228
3.670
10.371
-1.563
158.385
: OTL •
Total Vbl
440
440
440
440
440
440
440
440
440
440
roL
Used
340
340
340
340
340
340
340
340
340
340
. ' Wt.
RhalVdL
100
100
100
100
100
100
100
100
100
100
:;:jliufo>n.
' ^^aetox
1
1
1
1
1
1
1
1
1
1
Total wq
Result
< 0.647
< 0.129
< 0.129
< 0.129
1.99
12.6
0.475
1.34
< 0.518
20.5
Triangle Laboratories, Inc.
801 Capitola Drive * Durham, North Carolina 27713
Tele: (919) 544-5729 * Fax: (919) 544-5491
Printed: 30-M-97 at 10:21 AM
36
-------
Client: Eastern Research Group
Project Number: 42298
OA: Serial Dilution
Client Sample ID:
TLI Sample ID-
Date Prepared:
Date Analyzed:
Matrix'
LTV-88 & 2 & LTV -02. 101 FH
174-97-11. 1 & 173-60-1 A.10FH
Julv 18-25. 1997
Julv 28, 1997
Air
LTV-88 & 2 & LTV-02.101 FH L
174-97-11.1 & 173-60-1A.10FHL
Julv 18-25. 1997
Julv 28, 1997
Air
Analvte
As
Be
Cd
Co
Cr
Mn
Ni
Pb
Sb
Se
Native Sample
; Total, ug
; Result
4.63
< 0.100
72.7
< 0.100
21.7
53.5
81.8
15400
6.04
17.0
.:_"• ugfl.
: Core,
46.257
0.259
726.988
-7.271
216.987
535.365
817.800
30775.289
60.445
169.688
Serial Dilution
^i&aliig :
::"*:ftesult
3.96
< 0.500
76.6
< 0.500
24.5
54.2
86.3
15900
7.23
18.7
sg&,
G&nc,
7.927
0.136
153.150
-1.256
48.990
108.372
172.627
6354.457
14.467
37.387
; ' = ' RPB -
-------
Client: Eastern Research Group
Project Number: 42298
QA: Serial Dilution
Client Sample ID:
TLI Sample ID:
Date Prepared:
Date Analyzed'
Matrix:
LTV-03 BH
173-60-1B BH
Julv 18-25. 1997
Julv 28. 1997
Air
LTV-03 BH L
173-60-1B BH L
Julv 18-25. 1997
Julv 28. 1997
Air
Artalvte
As
Be
Cd
Co
Cr
Mn
Ni
Pb
Sb
Se
Native Sample
: Total ug; . .,..
; Rest*: :
< 0.588
< 0.118
0.695
< 0.118
2.98
11.9
4.51
8.44
< 0.470
19.8
••: ugfL.
: Cone,
0.216
0.205
5.910
-0.565
25.395
101.394
38.396
71.842
2.266
168.572
Serial Dilution
'• iTdtalug
: Result
< 2.94
< 0.588
0.658
< 0.588
3.27
11.7
4.61
10.9
< 2.35
21.6
! U^L
• Cbrib;-
-1.318
0.069
1.119
0.182
5.556
19.982
7.849
18.600
0.522
36.695
;HPD
-------
Client: Eastern Research Group
Project Number: 42298
QA: Duplicate
Client Sample ID:
TLI Sample ID:
Date Prepared:
Date Analvzed:
Matrix:
I TV-89 & 3 & LTV -08 FH
174-97-13.4 & 173-60-2A FH
Iiilv 18-25. 1997
Julv 28. 1997
Air
LTV-89 & 3 & LTV-08 FH DA
174-97-13.4 & 173-60-2A FH DA
Julv 18-25. 1997
Julv 28. 1997
Air
Analyte
As
Be
Cd
Co
Cr
Mn
Ni
Pb
Sb
Se
Sample
Tbtafcyg "v
- Rest* :^
433
< 0.100
67.5
< 0.100
17.2
56.1
117
15000
5.81
18.7
1 Ugt .
' "• " Cone.
43272
0.250
674.566
0.855
171.701
561.112
1166.381
15047.530
58.077
186.641
Duplicate
: , K-Teiaiug
;: : ftesult
4">8
< 0.100
67.0
0.117
17.1
55.9
116
15000
6.31
188
:. «gfl-
Conc.
42792
0.204
669.962
1.169
170.696
559.259
1160.938
14956.682
63.087
187.574
; RPD
-------
Client: Eastern Research Group
Project Number: 42298
QA: Duplicate
Client Sample ID:
TLI Sample ID:
Date Prepared:
Date Analyzed:
Matrix:
LTV-09 BH
173-60-2B BH
Julv 18-25. 1997
Julv 28. 1997
Air
LTV-09 BH DA
173-60-2B BH DA
Julv 18-25. 1997
Julv 28. 1997
Air
Analvte
As
Be
Cd
Co
Cr
Mn
Ni
Pb
Sb
Se
Sample
: ToMtig
Result
< 0.589
< 0.118
< 0.118
< 0.118
1.52
24.2
0.516
1.16
< 0.471
16.5
«*.
Cone.
-2.804
0.065
-0.318
-1.593
12.890
205.645
4.377
9.816
2228
139.641
Duplicate
: ,; Total yg
; Resaft
< 0.589
< 0.118
< 0.118
< 0.118
1.46
24.4
0.507
1.09
< 0.471
15.8
ugit
Cone.
-4576
0.081
-0.343
-1.807
12.366
206.673
4.301
9.255
1.696
134.400
FIFO,;
-------
Client: Eastern Research Group
Project Number: 42298
QA: Matrix Spikes (Post-Digestion)
Client Sample ID:
TLI Sample ID:
Date Prepared:
Dqtg Analyzed:
Matrix:
LTV-88 & 2 & LTV-02.101 FH PDS
174-97-11.1 & 173-60-1 A.10FHPDS
July 18-25, 1997
Julv 28. 1997
Air
AnaMe
As
Be
Cd
Co
Cr
Mn
Ni
Pb
Sb
Se
Post-Dig
ffeodvered:
Arnouikftia/LV
85.38
46.21
759.18
40.63
263.38
574.10
849.99
N/A
114.04
210.22
estion Spike
f • -,:-:f;SjpBg; •:•••:!•
':.'•'' fi?nX3UiAiix&$ '"• "•-'•"
50
50
50
50
50
50
50
N/A
50
50
::;./%
; fleccMsy
78°/<
92°/<
Spike Low
81°/<
93°/<
Spike Low
Spike Low
Spike Low
107°/<
81°/<
Post-Digestion Spike Duplicate
: Recovered^ ;:
Amount djtj/LV:
r ., Spite ..
> Amount (uq/U
"i %
RecowKV
RPD ;
--
—
—
--
--
—
—
--
—
—
—
—
—
—
—
—
—
—
—
—
—
~-
_
„
—
—
—
—
—
—
—
Triangle Laboratories, Inc.
801 Capitola Drive * Durham, NC 27713
Tele: (919) 544-5729 * Fax: (919) 544-5491
Printed: 30-M-97
at
09:37 AM
41
-------
Client: Eastern Research Group
Project Number: 42298
QA: Matrix Spikes (Post-Digestion)
Client Sample ID:
TLI Sample ID-
Date Prepared:
Date Analyzed:
Matrix:
LTV-03 BH PDS
173-60- 1BBHPDS
Tnlv 18-25. 1997
Julv 28. 1997
Air
Anafote
As
Be
Cd
Co
Cr
Mn
Ni
Pb
Sb
Se
Post-Dig
Recovered
Amourt&iaC.}
44.31
46.56
53.00
47.22
75.38
148.53
86.68
115.93
49.78
210.78
estion Spike
: Spike
Amoisit fao/U
50
50
50
50
50
50
50
50
50
50
-
%
i flecoweR?
89%
93%
94°/c
94°/<
100%
94%
97%
88%
100%
84%
Post-Digestion Spike Duplicate
Recovered
Amount ftkJ/Ll
•: vf".sps»: ••••
Amount (nest)
•• %
Fteeovery
• BPO
—
—
—
—
_
—
—
-
—
—
—
—
—
—
—
—
—
—
—
—
—
—
—
—
—
—
—
—
—
—
Triangle Laboratories, Inc.
801 Capitola Drive * Durham, NC 27713
Tele: (919) 544-5729 * Fax: (919) 544-5491
Printed: SO-Jul-97
at
09:37 AM
42
-------
Client: Eastern Research Group
Project Number: 42298
QA: Method Blank
TLI Samole ID:
Date Prepared:
Date Analyzed:
Matrix:
42298 MB
July 18-25, 1997
July 28, 1997
N/A
Anabjte
As
Be
Cd
Co
Cr
Mn
Ni
Pb
Sb
Se
Beeovemd:
AflK>yirt;fcKM
-5.10
029
-0.25
-0.48
-0.40
028
-1.28
1.18
0.54
121
Method Blank
:.::v: ! DeteeBort
^lii;&ti/U:
5
1
1
1
2
2
3
2
4
3
—
—
—
—
—
—
—
—
—
...
—
—
—
—
—
—
—
—
—
—
—
Pass or
Fail
Pass
Pass
Pass
Pass
Pass
Pass
Pass
Pass
Pass
Pass
—
—
—
—
—
—
—
—
—
—
—
—
—
—
—
—
—
—
—
—
—
Triangle Laboratories, Inc.
801 Capitola Drive * Durham, NC 2771
Tele: (919) 544-5729 * Fax: (919) 544-5491
Printed: 30-Jul-97
at
09:37 AM
43
-------
Client: Eastern Research Group
Project Number: 42298
QA: Lab Control Spikes
TLI Snmnle ID:
Date Prepared:
Date Analyzed:
Matrix:
42298 LCS
July 18-25. 1997
July 28. 1997
N/A
AnaJvte
As
Be
Cd
Co
Cr
Mn
Ni
Pb
Sb
Se
Lab Control Spike
Recovered
Amour* &ctfU.
41.89
44.31
45.10
46.55
46.66
45.99
45.33
52.49
52.65
44.65
: SpS«*.:. " v:
.flinourt&a&J.'^
50
50
50
50
50
50
50
50
50
50
: .::. */. . :..:•
;;• 7*. ..:..%;
84°/<
89°/<
90°/<
93°/<
93°/<
92°/
91°/<
1050/
105°/<
89°/<
Lab Control Spike Duplicate
,.-••• *«6GOVi6PBCr •
'. .:AB»ii*fQa!O:
-.;•' .;&*»• ;•
?: Atnbunt(oa£i
.- % '•
. ffeCGWKV
: RPD
—
—
—
—
—
—
—
—
—
—
—
—
—
—
—
—
—
—
—
—
—
—
—
—
—
—
—
—
—
—
—
Triangle Laboratories, Inc.
801 Capitola Drive * Durham, NC 27713
Tele: (919) 544-5729 * Fax: (919) 544-5491
Printed: 30-Jul-97
at
09:37 AM
44
-------
Client:
Project Number:
Sample Report
Eastern Research Group
42298
Page 1 of 6
)atc Received'
}ate Prf*nared'
)ate Analvzed*
)ATA FILE:
^atnv
JulvOl & 14. 1997
Tulv 18-29. 1997
Julv 21 & 29-31. 1997
AB780. AB785 & AB787
Air
ANALYTE Ha
ua/LRDL 0.2
Analysis Method:
29
Instrument P E Zeeman 5100
Soike Cone. (uo/U
CVAA ANALYTE SUMMARY REPORT
3«ntSafnpfe&>
LTV-88&2<V-02FH
LTV-88&2<V-02FHD
LTV-03BH
LTV-03 BH D
LTV-04 HNO3
LTV-04 HNO3 D
LTV-05 KMnO4
LTV-05 KMnO4 D
LTV-06 Hd
LTV-06 HCI D
LTV-S9&3<V-08FH
LTV-89 & 3 & LTV-08 FH D
LTV-09BH
LTV-09 BH D
LTV-10 HNO3
LTV-10 HNO3 D
LTV-11KMn04
LTV-11 KMnO4D
LTV-12HCI
LTV-12HCID
LTV-90&4<V-14FH
LTV-90&4<V-14FHD
LTV-15 BH
LTV-15 BH D
LTV-16 HNO3
LTV-16 HNO3 D
LTV-17 KMnO4
LTV-17 KMnO4 D
LTV-18HCI
.TV-18HCID
TLJ3AMP1D
174-97-11,1 & 173-60-1A.10
174-97-11,1 4 173-60-1A.10D
1 73-60-1 B
1 73-60-1 BD
1 73-60-1 C
173-60-1CD
1 73-60-1 D
173-60-100
1 73-60-1 E
173-60-1 ED
174-97-1 3,4 &173-60-2A
174-97-13,4 & 173-60-2A D
173-60-2B
173-60-2BD
173-60-2C
173-60-2CD
173-60-20
173-60-200
173-60-2E
173-60-2ED
174-97-1 5,6 &173-60-3A
174-97-1 5,6 &173-60-3AD
173-60-38
173-60-3BD
173-60-3C
173-60-3CD
173-60-30
173-60-300
173-60-3E
173-60-3ED
ug&.
-------
Client:
Project Number;
Eastern Research Group
42298
Sample Report
Page 2 of 6
! Date Received:
!Date Prepared:
!Date A^nalvzed*
iDATA FILE:
I Matrix:
Julv 01 & 14. 1997
Julv 18-29. 1997
Julv 21 & 29-11. 1997
AB780, AB785 & AB787
Air
ANALYTE: Ho
uo/LRDL 0.2
Anah/sis Method-
29
Instrument P E Zeeman 5100
Sake Cone. (uo/TJ 5
CVAA ANALYTE SUMMARY REPORT
CfemSamc*»«3
1 LTV-39 & 8 & LTV-38 FH
LTV-39 & 8 & LTV-38 FH D
1 LTV-38,40 BH
LTV-38,40 BH D
LTV-41 HNO3
LTV-41 HNO3 D
LT\M2 KMnO4
LTV-42 KMnO4 D
LTV-42,43 HCI
LTV-42,43 HCI D
LTV-52&10<V-51FH
LTV-52&10<V-51 FH D
: LTV-51,53BH
LTV-51.53BHD
1 LTV-54 HNO3
LTV-54 HNO3 D
r LTV-55 KMnO4
LTV-55 KMnO4 D
"" LTV-55,56 HCI
LTV-55,56 HCI D
LTV-58FH -,. - •'"
LTV-58 FH D
LTV-58.60BH ,'-, -•'-',
LTV-58,60 BH D
LTV-58 HNO3 , , .
LTV-58 HN03D -<: '."'">
LTV-61 KMnO4
LTV-61 KMnO4 D
LTV-61.62HCI
LTV-61, 62 HOD
TttSAMPtB
174-97-18,8 4 173-60-4A
174-97-18,8 & 173-60-4A D
173-60-4AB
173-6CWAB D
173-60-4C
173-60-4C D
173-60-4D
173-60-4D D
173-6CWDE
173-60-4DE D
174-97-1 9,9 &173-60-5A
174-97-19,9 & 173-60-5A D
173-60-5AB
173-60-5AB D
173-60-5C
173-60-5C D
173-60-5D
173-60-5D D
173-60-5DE
173-60-5DE D
173-60-6A
173-60-6A D
173-60-6AC
173-60-6AC D
173-60-6A Hg
173-60-6A Hg D
173-60-6D
173-60-6D D
173-60-6DE
173-60-6DE D
«*.
CC»C
0.039
0.023
0.003
0.000
0.003
0.008
0.065
0.091
0.013
0.010
0.023
0.013
0.039
0.029
0.021
0.021
0.029
0.023
0.037
0.029
0.025
0.013
0.039
0.026
0.023
0.029
0.154
0.081
0.018
0.021
m
w
N/A
N/A
300
300
33
33
260
260
65
65
N/A
N/A
300
300
65
65
275
275
75
75
N/A
N/A
150
150
100
100
95
95
220
220
ntf
FSf
100
100
N/A
N/A
N/A
N/A
N/A
N/A
N/A
N/A
100
100
N/A
N/A
N/A
N/A
N/A
N/A
N/A
N/A
100
100
N/A
N/A
N/A
N/A
N/A
N/A
N/A
N/A
fl*
Afctutt
5
5
5
5
5
5
5
5
5
5
5
5
5
5
5
5
5
5
5
5
5
5
5
5
5
5
5
5
5
5
at
FACH3F
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
, mtaa
- flESULT
< 0.400
< 0.400
< 1.20
< 1.20
< 0.132
< 0.132
< 1.04
< 1.04
< 0260
< 0260
< 0.400
< 0.400
< 1.20
< 1.20
< 0260
< 0260
< 1.10
< 1.10
< 0.300
< 0.300
< 0.400
< 0.400
< 0.600
< 0.600
< 0.400
< 0.400
< 0.380
< 0.380
< 0.880
< 0.880
Am
RESULT
< 0.400
< 1.20
< 0.132
< 1.04
< 0.260
< 0.400
< 1.20
< 0.260
< 1.10
< 0.300
< 0.400
< 0.600
< 0.400
< 0.380
< 0.880
RPB
_
_
-
_
-
-
_
-
_
-
-
-
-
-
-
%REC
_
-
-
_
-
-
-
-
-
-
-
-
-
-
-
46
-------
Client:
Project Number:
Eastern Research Group
42298
Sample Report
Page 3 of 6
Date Received:
Date Prenared:
Date Analvzed:
DATA FILE:
Matrix:
Julv 01 & 14. 1997
Julv 18-29. 1997
Julv 21 & 29-31. 1997
AB780, AB785 & AB787
Air
ANALYTE: Ho
uo/L RDL 0.2
Anaivsis Method:
29
Instrument P E Zeeman 5100
Snika Cone. fiio/D 5
CVAA ANALYTE SUMMARY FEPORT
^tS*nDfe.iD
LTV-57BH i • ;. i j-C',
LTV-57BHD r" " ' •
LTV-59 KMnO4
LTV-59 KMnO4 D
LTV-46& 9 & LTV-45 FH
LTV-46 & 9 & LTV-45 FH D
LTV-45,47 BH
LTV-45,47 BH D
LTV-45 HNO3 ,- , . .--
LTV-45 HNO3 D '-"
LTV-48 KMnO4
LTV-48 KMn04 D
LTV-48,49 HCI
LTV-48,49 HCI D
LTV-91,99 & 5,12 & LTV-20 FH
LTV-91,99 & 5,12 & LTV-20 FH D
LTV-21 BH
LTV-21 BH D
LTV-22 HNO3
.TV-22 HNO3 D
-TV-23 KMnO4
-TV-23 KMnO4 D
-TV-24 HCI
JV-24 HCI D
TtSSAMRD
173-60-7
173-60-70
173-60-6B
1 73-60-68 D
1 74-97-20, 1 0 & 1 73-60-1 1 A
174-97-20,10 & 173-60-11AD
1 73-60-1 1AB
173-60-11 ABO
173-60-11 A
173-60-11AD
173-60-110
173-60-110 D
1 73-60-1 1DE
1 73-60-1 1DED
174-97-1 2,1 7,2,3 & 173-60-12A
1 74-97-1 2, 1 7,2,3 & 1 73-60-1 2A D
173-60-12B
1 73-60-1 2BD
173-60-12C
173-60-12C D
73-60-120
73-60-120 D
73-60-1 2E
73-60-12E D
; SONG
0.047
0.060
0.021
0.021
0.023
0.026
0.029
0.018
0.013
0.013
0.047
0.078
0.037
0.016
0.146
0.149
0.056
0.069
0.311
0.301
0.039
0.042
-0.005
-0.002
mi
TV
200
200
220
220
N/A
N/A
150
150
20
20
90
90
90
90
N/A
N/A
610
610
90
90
210
210
70
70
a*
N/A
N/A
N/A
N/A
100
100
N/A
N/A
N/A
N/A
N/A
N/A
N/A
N/A
100
100
N/A
N/A
N/A
N/A
N/A
N/A
N/A
N/A
m
A&fttt
5
5
5
5
5
5
5
5
5
5
5
5
5
5
5
5
5
5
5
5
5
5
5
5
-m.
factcs
1
1
1
1
1
1
1
1
i
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
msm
< 0.800
< 0.800
< 0.880
< 0.880
< 0.400
< 0.400
< 0.600
< 0.600
< 0.080
< 0.080
< 0.360
< 0.360
< 0.360
< 0.360
< 0.400
< 0.400
< 2.44
< 2.44
0.560
0.542
< 0.840
< 0.840
< 0.280
< 0.280
KiK
_
< 0.800
__
< 0.880
_
< 0.400
< 0.600
< 0.080
< 0.360
_
< 0.360
_
< 0.400
^
< ''2.44
0.551
_
< 0.840
< 0.280
ife
_
-
_
-
-
-
-
-
_
-
_
-
-
_
—
-
-
fc^REd
-
_
-
-
-
-
-
-
-
_^ _
\ _
_
y
_
-
-
47
-------
Client:
Project Number:
Eastern Research Group
42298
Sample Report
Page 4 of 6
Date Received:
Dale Prepared:
Date Analyzed:
DATA FILE:
Matrix:
JulvOl & 14. 1997
Julv 18-29. 1997
Julv 21 & 29-31. 1997
AB780, AB785 i AB787
Air
ANALYTE: Ho
uo/L RDL 0.2
Analysis Metrxxt
29
Instrument P E Zeeman 5100
Spike Cone. iua/L) 5
CVAA ANALYTE SUMMARY REPORT
CtKsntSampfelO
LTV-92 & 6 & LTV-26 FH
LTV-92&6<V-26FHD
LTV-27 BH
LTV-27 BH D
LTV-28 HNO3
LTV-28 HNO3 D
LTV-29 KMnO4
LTV-29 KMnO4 D
LTV-30 HCI
LTV-30 HCI D
LTV-93 & 7 & LTV-32 FH
LTV-93&7<V-32FHD
LTV-33BH
LTV-33 BH D
LTV-34 HNO3
LTV-34 HNO3 D
LTV-35 KMnO4
LTV-35 KMnO4 D
LTV-36 HCI
LTV-36 HCI D
LTV-03 BH MS
LTV-03 BH MSD
LTV-09 BH MS
LTV-09 BH MSD
LTV-15BHMS
LTV-15BHMSD
LTV-90 & 4 & LTV-14 FH MS
LTV-90 & 4 & LTV-14 FH MSD
LTV-61.62HCIMS
LTV-61.62HCIMSD
TtJSAMttD ~*
174-97-1 4,5 4 173-60-13A
174-97-14,5 & 173-60-1 3A D
173-60-13B
173-60-13BD
1 73-60-1 3C
173-60-13CD
173-60-1 3D
173-60-1 3D D
173-60-13E
1 73-60-1 3E D
174-97-16,7 & 173-60-14A
174-97-16,7 & 173-60-14A D
1 73-60-1 4B
1 73-60-1 4BD
173-60-14C
1 73-60-1 4C D
173-60-140
1 73-60-1 4D D
1 73-60-1 4E
173-60-14ED
173-60-18 MS
1 73-60-1 B MSD
173-60-2BMS
173-60-2B MSD
173-60-3BMS
173-60-3BMSD
1 74-97-15,6 & 173-60-3A MS
174-97-15,6 & 173-60-3A MSD
173-60-6DEMS
173-60-6DEMSO
>&
XAJP&x
0527
0542
0.127
0.137
-0.015
-0.022
0.007
0.007
0.002
-0.002
0.276
0.271
0.125
0.130
0.015
0.000
0.054
0.054
0.002
0.005
5.183
5572
5.186
4.982
5.113
5.454
4.735
4.988
5.316
5564
Rtf '
m
N/A
N/A
440
440
60
60
255
255
65
65
N/A
N/A
440
440
50
50
260
260
95
95
670
670
660
660
690
690
N/A
N/A
220
220
fltlt.:
:,fV:'
100
100
N/A
N/A
N/A
N/A
N/A
N/A
N/A
N/A
100
100
N/A
N/A
N/A
N/A
N/A
N/A
N/A
N/A
N/A
N/A
N/A
N/A
N/A
N/A
100
100
N/A
N/A
%v«alx:-
?A»5U
-------
lent:
•oiect Number:
Eastern Research Group
422??
ample Report
Page 5 of 6
•e Received-
'e Prepared'
re \nalv7ed"
T\ FILE-
tnx:
TiilvOI A 14 1997
Julv 18-29. 1997
Julv21 & 29-11. 1997
AB780. AB785 &AB787
Air
ANALYTE: Hg
uq/L RDL 0.2
Analysis Method:
29
Instrument P E Zeerr)an 5100
Soika Cone. (uo/U
5
CVAA ANALYTE SUMMARY REPORT
sitSarnofatD
"V-21 BH MS
"V-21 BH MSD
"V-27 BH MS
V-27 BH MSD
V-33 BH MS
V-33 BH MSD
V-03 BH MS
V-03 BH MSD
V-09 BH MS
V-09 BH MSD
V-15BHMS
V-15 BH MSD
V-90&4<V-14FHMS
V-90&4<V-14FHMSD
V-61.62HCIMS
V-61.62HCIMSD
V-21 BH MS
V-21 BH MSD
V-27 BH MS
V-27 BH MSD
V-33 BH MS
V-33 BH MSD
hod Blank
led Blank D
iD
«>'
TySAMPlO
173-60-1 26 MS
173-60-12B MSD
1 73-60-1 3B MS
1 73-60-1 3B MSD
1 73-60-1 4B MS
1 73-60-1 4B MSD
True Spike MS
True Spike MSD
True Spike MS
True Spike MSD
True Spike MS
True Spike MSD
True Spike MS
True Spike MSD
True Spike MS
True Spike MSD
True Spike MS
True Spike MSD
Tiue Spike MS
True Spike MSD
True Spike MS
True Spike MSD
42298 MB1
42298 MB1 D
42298 LCS1
42298 LCS1 D
wrt.
CGNC
4.069
3.787
4.808
5.116
5.077
5.170
5
5
5
5
5
5
5
5
5
5
5
5
5
5
5
5
0.024
0.012
6.258
5.882
Brtt
TV
610
610
440
440
440
440
670
670
660
660
690
690
N/A
N/A
220
220
610
610
440
440
440
440
-
-
ml
&f
N/A
N/A
N/A
N/A
N/A
N/A
N/A
N/A
N/A
N/A
N/A
N/A
100
100
N/A
N/A
N/A
N/A
N/A
N/A
N/A
N/A
_
-
* fltf
A&wot
5
5
5
5
5
5
5
5
5
5
5
5
5
5
5
5
5
5
5
5
5
5
-
-
8&
exxof
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
-
-
Tetetis
RE&JL1
49.6
462.
42.3
45.0
44.7
45.5
67.0
67.0
66.0
66.0
69.0
69.0
10.0
10.0
22.0
22.0
61.0
61.0
44.0
44.0
44.0
44.0
-
-
A»0»
13B9ULT
47.9
43.7
45.1
67.0
66.0
69.0
10.0
22.0
61.0
44.0
44.0
-
-
.8PB.
7.18%
651%
1.82%
-
-
-
-
-
-
-
-
-
-
%R£C
81%
76%
96%
102%
102%
103%
-
-
-
-
-
-
-
-
-
125%
118%
49
-------
Client:
Project Number:
Eastern Research Group
42298
Sample Report
Page 6 of 6
Dale Received:
Date Prepared:
Date Analvzed:
DATA FILE:
Matrix:
Julv 01 & 14. 1997
Julv 18-29. 1997
Julv 21 & 29-31. 1997
AB780, AB785 &. AB787
Air
ANALYTE Hq
uq/L RDL- 02
Anarvsts Method:
29
Instrument P E Zeeman 5100
Spike Cone. (ug/U
5
CVM ANALYTE SUMMARY REPORT
QtatSttM
Method Blank
Method Blank D
LCS
LCSD
Method Blank
Method Blank D
LCS
LCSD
Method Blank
Method Blank D
LCS
LCSD
TtJSAMPfB ' ' ' %&' ' .
42298 MB2
42298 MB2D
42298 LCS2
42298 LCS2D
42298 MBS
42298 MBS D
42298 LCS3
42298 LCS3D
42298 MB4
42298 MB4D
42298 LCS4
42298 LCS4D
'CQNC
0.029
0.018
4.928
4.784
0.016
0.008
5546
4.949
0.003
-0.003
4.592
4.980
:. oik
-
—
-
—
-
-
'&
:
_
_
_
-
-
A*J»I
:
_
_
_
-
-
,vSfc,
JwEwpQl'
:
_
—
_
_
-
MfetiB
-
-
-
-
-
-
:
-
_
-
_
-
:
_
-
-
-
-
-
99%
96%
-
105%
99%
-
92%
100%
Triangle Laboratories, Inc.
801 Capitola Drive * Durham, North Carolina 27713
Tele: (919) 544-5729 * Fax: (919) 544-5491
Printed: 01-Aug-97 at 12:51 PM
50
-------
LTV STEEL COMPANY
CHAIN OF CUSTODY
I
RELINQUISHED BY = 1 {_! .. Q' [ . < DATE = . ^.A^ ' 1 / *» T* RECEIVED BY: (V
RELINQUISHED BY- !\V)/l[ f f?X \ .A .^UX, DATE = /I, / 1' J v /l/,/^"? RECEIVED BY: /
SAMPLE ID
i-H.TV-88
^ LTV-91
^LTV-89
--^LTV-92
<- LTV-90
— LTV-93
*-~~LTV-99
u-LTV-39
""lTV-52
<-lTV-46
I W I -•' ' (
\J FIELD ID
LTV- 062497- M29- OUTLET- F- 1
LTV- 062497- M29- INLET- F- 1
LTV- 062697- M29- OUTLET- F- 2
LTV- 062697- M29- INLET- F- 2
LTV- 062797- M29- OUTLET- F- 3
LTV- 062797- M29- INLET- F- 3
LTV- 062597- M29- INLET- F- 1A
LTV- 062697- M29- OUTLET- F- FBI
LTV- 062697- M29- INLET- F- FB2
LTV- 062497- M29- OUTLET- F- RB1
^ SAMPLE TYPE
METHOD 29, OUTLET, RUN 1
METHOD 29, INLET, RUN 1
METHOD 29, OUTLET, RUN 2
METHOD 29, INLET, RUN 2
METHOD 29, OUTLET, RUN 3
METHOD 29, INLET, RUN 3
METHOD 29. INLET, RUN 1
METHOD 29, OUTLET, FB1
METHOD 29, INLET, FB2
METHOD 29, OUTLET, RB1
f\ /\ *fl
Yv 1 /^ /^~\ >\
1 1 \LI nA/M/V^ DATE: ,
" DATE: (
fcjll.Jir
PRESERVATIVE
S Filter
i Filter ( 1 of 2)
Filter
Filter
" Filter
y Filter
Filter (2 of 2)
FILTER
^ FILTER
^ FILTER
U (U-V / , /^ r/
/ '
COMMENTS
#002
#007
#009
#023
#018
#008
#024
#011
#010
#024
ANALYSIS
Metals
Mtlals
Metals
Metals
Metals
Metals
Metals
Metals
Metals
Metals
7
CJ1
Page 2
-------
LTV STEEL COMPANY
CHAIN OF CUSTODY
RELINQUISHED BY- ,
RELINQUISHED BY - 1
q,.Q;, «
AVlV/Vl^
. ,^1.^1/f- DATE =
i/i^. DATE »
iq_G^ 1 , I <=r<,-T-
.li/ta* "/V,/?? 7
RECEIVED BY: •'
RECEIVED BY: 7
> — ' •— - /^/
' f ' C-4-?A A./Q{/*/\ DATE : J
IAA Lu
{.it
DATE:// / '
jSt>ci.Kf-<-v:*fc
SAMPLE ID
LTV-01
LTV-19
LTV- 100
LTV-07
LTV-25
LTV-13
LTV-31
LTV-37
LTV-50
LTV-44
LTV-83
FIELD ID
LTV- 062497- M29- OUTLET- APR- 1
LTV- 062497- M29- INLET- APR- 1
LTV- 062597- M29- INI ET- APR- 1A
LTV- 062697- M29- OUTLET- APR- 2
LTV- 062697- M29- INLET- APR- 2
LTV- 062797- M29- OUTLET- APR- 3
LTV- 062797- M29- INLET- APR- 3
LTV- 062697- M29- OUTLET- APR- FB1
LTV- 062697- M29- INLET- APR- FB2
LTV- 062497- M29- OUTLET- APR- RB1
LTV- 062497- M23- OUTLET- PR- RB1
° SAMPLE TYPE
METHOD 29. OUTLET, RUN 1
METHOD 29. INLET, RUN 1
METHOD 29, INI ET, RUN 1
METHOD 29, OUTLET, RUN 2
METHOD 29, INLET, RUN 2
METHOD 29, OUTLET, RUN 3
METHOD 29, INLET, RUN 3
METHOD 29, OUTLET, FB1
METHOD 29, INLET, FB2
METHOD 29, OUTLET, RB1
METHOD 23. OUTLET, RB 1
PRESERVATIVE
ACETONE PROBE RINSE
ACETONE PROBE RINSE
ACETONE PROBE RINSE
ACETONE PROBE RINSE
ACETONE PROBE RINSE
ACETONE PROBE RINSE
ACETONE PROBE RINSE
ACETONE PROBE RINSE
ACETONE PROBE RINSE
ACETONE
Acetone Probe Rinse
-COMMENTS
2 »-
5 (1 of 2) "
12 (2 of 2) w
3 «_
6 ^
4 ^-^
~j
o t^*
10 '-—
9 —
ANALYSIS
- Metals
Metals
Metals
Meldlb
Metals
Metals
' Metals
Metals
Metals
' Metals
DIoxms/PAH
ft
7/
ut
ro
Page 2
-------
LTV STEEL COMPANY
CHAIN OF CUSTODY
RELINQUISHED BY-
RELINQUISHED BY'
DATE'
DATE'
i,
RECEIVED BY:.
RECEIVED BY:
6
: 7 //
DATE:
SAMPLE ID
LTV-02
LTV-20
LTV-101
LTV-08
LTV-26
LTV-14
LTV-32
LTV-38
LTV-51
LTV-96
LTV-87
LTV-45
LTV-58
FIELD ID
LTV- 062497- M29- OUTLET- HN- 1
LTV- 062497- M29- INLET- HN- 1
LTV- 062597- M29- INLET- HN- 1A
LTV- 062697- M29- OUTLET- HN- 2
LTV- 062697- M29- INLET- HN- 2
LTV- 062797- M29- OUTLET- HN- 3
LTV- 062797- M29- INLET- HN- 3
LTV- 062697- M29- OUTLET- HN- FB1
LTV- 062697- M29- INLET- HN- FB2
LTV- 062597- M29- OUTLET- HNO- PB
LTV- 062687- M29- INLET- HNO- PB
LTV- 062497- M29- OUTLET- HNO- RBI
LTV- 062697- M29- INLET- HNO- RB2
SAMPLE TYPE
METHOD 29, OUTLET, RUN 1
METHOD 29, INLET, RUN 1
METHOD 29, OUTLET, RUN 1
METHOD 29, OUTLET, RUN 2
METHOD 29, INLET, RUN 2
METHOD 29, OUTLET, RUN 3
METHOD 29, INLET, RUN 3
METHOD 29, OUTLET, FB1
METHOD 29, INLET, FB2
METHOD 29. OUTLET, PROOF BLANK
METHOD 29, INTLET, PROOF BLANK
METHOD 29, OUTLET, RBI
METHOD 29, INLET, RB2
PRESERVATIVE
NITRIC ACID PROBE RINSE
NITRIC ACID PROBE RINSE
Nitric Acid Probe Rinse
NITRIC ACID PROBE RINSE
NITRIC ACID PROBE RINSE
NITRIC ACID PROBE RINSE
NITRIC ACID PROBE RINSE
NITRIC ACID PROBE RINSE
NITRIC ACID PROBE RINSE
0.1NHNO3 Rinse
0.1NHNO3Rln»«
0.1NHNO3
0.1NHN03
COMMENTS
* "K7-
B — ~
\ S\ 7, >
4-% — ! —
1
\*
v»
ANALYSIS
Metals
Metals
Metals
Metals
Metals
Metals
Metals
Metals
Metals
>** Metair*
,vAOW«tr"
Metals
Metals
CO
Paged
-------
LTV STEEL COMPANY
CHAIN OF CUSTODY
RELINQUISHED BY =
RELINQUISHED BY -
O
DATE'
DATE'
RECEIVED BY: ff> W*TsT/2^~
RECEIVED BY:
DATE:.
DATE:
SAMPLE ID
LTV-05
LTV-23
LTV-1 1
LTV-29
LTV-1 7
LTV-35
LTV-42
LTV-55
LTV-48
LTV-61
FIELD ID
LTV- 062497- M29- OUTLET- KMnO- 1
LTV- 062497- M29- INLET- KMnO- 1
LTV- 062697- M29- OUTLET- KMnO- 2
LTV- 062697- M29- INLET- KMnO- 2
LTV- 062797- M29- OUTLET- KMnO- 3
LTV- 062797- M29- INLET- KMnO- 3
LTV- 062697- M29- OUTLET- KMnO- FB1
LTV- 062697- M29- INLET- KMnO- FB2
LTV- 062497- M29- OUTLET- KMnO- RB1
LTV- 062597- M29- INLET- KMnO- RB2
SAMPLE TYPE
METHOD 29, OUTLET, RUN 1
METHOD 29, INLET, RUN 1
METHOD 29, OUTLET, RUN 2
METHOD 29, INLET, RUN 2
METHOD 29, OUTLET, RUN 3
METHOD 29, INLET, RUN 3
METHOD 29, OUTLET. FB1
METHOD 29, INLET, FB2
METHOD 29, OUTLET, RB1
METHOD 29. INLET, RB2
PRESERVATIVE
KMnO4 IMPINGERS
KMnO4 IMPINGERS
KMn04 IMPINGERS
KMn04 IMPINGERS
KMnO4 IMPINGERS
KMnO4 IMPINGERS
KMnO4 IMPINGERS
KMnO4 IMPINGERS
KMn04
KMnO4
COMMENTS
ANALYSIS
Metals
Metals
Metals
Metals
Metals
Metals
Metals
Metals
Metals
Metals
y
01
Page 7
-------
LTV STEEL COMPANY
CHAIN OF CUSTODY
RELINQUISHED BY'
RELINQUISHED BY'
.-0 <-J
DATE'
DATE'
RECEIVED BY:
RECEIVED BY:
DATE:
DATE:
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SAMPLE ID
LTV-03
LTV-21
LTV-09
LTV-27
LTV-15
LTV-33
LTV-40
LTV-53
LTV-47
LTV-60
LTV-04
LTV-22
LTV-10
LTV-28
LTV-16
LTV-34
LTV-41
LTV-54
FIELD ID
LTV- 062497- M29- OUTLET- BH- 1
LTV- 062497- M29- INLET- BH- 1
LTV- 062697- M29- OUTLET- BH- 2
LTV- 062697- M29- INLET- BH- 2
LTV- 062797- M29- OUTLET- BH- 3
LTV- 062797- M29- INLET- BH- 3
LTV- 062697- M29- OUTLET- BH- FB1
LTV- 062697- M29- INLET- BH- FB2
LTV- 062497- M29- OUTLET- BH- RB1
LTV- 062597- M29- INLET- BH- RB2
LTV- 062497- M29- OUTLET- BHM- 1
LTV- 062497- M29- INLET- BHM- 1
LTV- 062697- M29- OUTLET- BHM- 2
LTV- 062697- M29- INLET- BHM- 2
LTV- 062797- M29- OUTLET- BHM- 3
LTV- 062797- M29- INLET- BHM- 3
LTV- 062697- M29- OUTLET- BHM- FBI
LTV- 062697- M29- INLET- BHM- FB2
SAMPLE TYPE
METHOD 29, OUTLET, RUN 1
METHOD 29, INLET, RUN 1
METHOD 29, OUTLET, RUN 2
METHOD 29, INLET, RUN 2
METHOD 29, OUTLET, RUN 3
METHOD 29, INLET, RUN 3
METHOD 29, OUTLET, FB1
METHOD 29, INLET, FB2
METHOD 29, OUTLET, RB1
METHOD 29, INLET, RB2
METHOD 29, OUTLET, RUN 1
METHOD 29, INLET, RUN 1
METHOD 29, OUTLET, RUN 2
METHOD 29, INLET, RUN 2
METHOD 29, OUTLET, RUN 3
METHOD 29, INLET, RUN 3
METHOD 29, OUTLET, FB1
METHOD 29, INLET, FB2
PRESERVATIVE
HNO3/H2O2 BACK HALF
HNO3/H2O2 BACK HALF
HNO3/H2O2 BACK HALF
HNO3/H2O2 BACK HALF
HNO3/H2O2 BACK HALF
HN03/H2O2 BACK HALF
HN03/H2O2 BACK HALF
HN03/H202 BACK HALF
HNO3/H202
HNO3/H2O2
0.1 NHNO3 RINSE - Hg
0.1 NHN03 RINSE - Hg
0.1 NHNO3 RINSE - Hg
0.1 NHNO3 RINSE- Hg
0.1 NHN03 RINSE -Hg
0.1 NHN03 RINSE - Hg
0.1 NHNO3 RINSE -Hg
0.1 NHN03 RINSE -Hg
COMMENTS
ANALYSIS
Metals
Metals
Metals
Metals
Metals
Metals
Metals
Metals
Metals
Metals
Metals
Metals
Metals
Metals
Metals
Metals
Metals
I
u\
Page 3
-------
LTV STEEL COMPANY
CHAIN OF CUSTODY
RELINQUISHED BY -
RELINQUISHED BY"
DATE'
DATE'
RECEIVED BY:.
RECEIVED BY:
DATE:
DATE:
•^
V
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SAMPLE ID
LTV-06
LTV-24
LTV-12
LTV-30
LTV- 18
LTV-36
LTV-43
LTV-56
LTV-49
LTV-62
FIELD ID
LTV- 062497- M29- OUTLET- HCI- 1
LTV- 062497- M29- INLET- HCI- 1
LTV- 062697- M29- OUTLET- HCI- 2
LTV- 062697- M29- INLET- HCI- 2
LTV- 062797- M29- OUTLET- HCI- 3
LTV- 062797- M29- INLET- HCI- 3
LTV- 062697- M29- OUTLET- HCI- FB1
LTV- 062697- M29- INLET- HCI- FB2
LTV- 062497- M29- OUTLET- HCI- RB1
LTV- 062797- M29- INLET- HCI- RB2
SAMPLE TYPE
METHOD 29, OUTLET, RUN 1
METHOD 29, INLET. RUN 1
METHOD 29, OUTLET, RUN 2
METHOD 29, INLET, RUN 2
METHOD 29, OUTLET, RUN 3
METHOD 29, INLET, RUN 3
METHOD 29, OUTLET, FB1
METHOD 29, INLET, FB2
METHOD 29, OUTLET, RB1
METHOD 29, INLET, RB2
PRESERVATIVE
8N HCI RINSE - Hg
8N HCI RINSE - Hg
8N HCI RINSE - Hg
8N HCI RINSE - Hg
8N HCI RINSE - Hg
8N HCI RINSE - Hg
8N HCI RINSE - Hg
8N HCI RINSE - Hg
8NHCI
8NHCI
COMMENTS
ANALYSIS
Metals
Metals
Metals
Metals
Metals
Metals
Metals
Metals
Metals
Metals
en
PageS
-------
|| Custody Seal :
|| Chain of Custody :
|| Sample Tags :
U Sample Tag Numbers:
II . SMO Forms :
II Box
Absent
Present
Absent
Not Listed
N/A
Sample Seals: Absent
Container...: Intact
on Chain of Custody
NO COOLANT
TLI Project Number 42298
Client: ERGO 2 - Eastern Research Group
s\
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Date Received |
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Carrier and Number |
07/01/97 | By //yy
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||173-60-1A LTV-02 NITRIC ACID|
(I LTV- 02 METALS LAB j
1
IJ173-60-1B LTV-03 HN03/H202|
\ LTV-03 METALS LAB j
1
||173-60-1C LTV-04 0.1NHN03|
Jl LTV-04 METALS LAB 41 |
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||173-60-1D LTV-OS KMN04|
|j LTV-05 METALS LAB,
-------
jj Custody Seal : Absent Sample Seals: Absent
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||TLI Number Client Sample ID . Matrix) To LAB
j|mR/H-CPM Client COC ID • Location | Date/Init
||173-60-3E LTV-18 8N HC1 1
|| LTV-18 METALS LAB j
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II - 1
||173-60-4A LTV-38 NITRIC ACID|
|| LTV-38 METALS LAB j
II 1 1
gi73-60-4B LTV-40 HN03/H202|
j LTV-40 METALS LAB |
||173-60-4C LTV-41 0 . IN HN03 1
H LTV-41 METALS LAB Un |
||173-60-4D LTV-42 KMN04 j
g LTV-42 METALS LAB j
||
II
||173-60-4E LTV-43 8NHC1 1
|| • LTV-43 METALS LAB j
II
gi73-60-5A LTV-51 NITRIC ACID)
|| LTV-51 METALS LAB j
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gi73-60-5B LTV-53 HN03/H202|
H LTV-53 METALS LAB j
II I
gi73-60-5C LTV-54 0 . IN HN03 1
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|173-60-5E LTV-S6 8N HC1 |
|j LTV-56 METALS LAB j
II 1
gi73-60-6A LTV-5B NITRIC ACIDJ
|| . LTV- 58 METALS LAB |
II 1
||173-60-6B LTV-59 i^fol ^ KW*'HW'A
LTV- 5 9 «\\1 ' METALS LAB j
173-60-6C LTV-60 C0&1 ^V^\»'"' IB'W I
LTV- 60 irtYZfA^' METALS Lts 1
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=Form Revised 05/27/1997 -- Page 2 OF 3=
-------
|| Custody Seal : Absent Sample Seals: Absent
|| Chain of Custody : Present Container...: Intact
(I Sample Tags : Absent
|| Sample Tag Numbers: Not Listed on Chain of Custody
II SMO Forms : N/A
TLI Project Number 42298 Book ||
Client: ERG02 - Eastern Research Group |j
173 ||
1 I l\/\
Date Received | 07/01/97 | By / //J/l-xx/^ Pa9e II
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|| Box NO COOLANT Carrier and Number | JIM GAUGHEY I/ 60 y
||TLI Number Client Sample ID Matrixj To LAB
||mR/H:CPM. Client COC ID . . * Location | Date/Init
JJ173-60-6D LTV-61 KMN04 |
I) LTV-61 METALS LAB j
II 1
||173-60-6E LTV-62 8N HC1 1
II LTV-62 METALS LAB j
II 1
IJ173-60-7 LTV-57 . H202/HN03 1
y LTV-57 METALS LAB |
II 1
yi73-60-8 LTV- 96 0.1N HN03|
IJ LTV- 96 METALS LAB |
||l73-60-9 LTV-97 0.1NHN03J
I) LTV-97 METALS LAB |
»|
||173-60-10 LTV-101 0.1N HN03PR|
U LTV-101 METALS LAB j
||173-60-11A LTV-45 0 . IN HN03PR)
|| LTV-45 METALS LAB j
II 1
II 1
||173-60-11B LTV-47 HN03/H202|
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||173-60-11C LTV-87 ^^§Vfl HllOj IMP'
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||173-60-11D LTV-48 KMNU4 1
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H173-60-11E LTV-49 8N HC1 1
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||173-60-12A LTV-20 NITRIC ACIDJ
|| LTV-20 METALS LAB j
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||173-60-12B LTV-21 HN03/H202)
|| LTV-21 METALS LAB |
1
||173-60-12C LTV-22 0 . IN HN03 1
|| LTV-22 METALS LAB Un j
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Date/Init
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Date/Init
To STORAGE |
Date/Init
To LAB
Date/Init
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Date/Init
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Date/Init
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Ol
CD
-------
=TRIANQLE LABORATORIES, INC. -- LOG IN RECORD/CHAIN OF CUSTODY-
Custody Seal : Absent
Chain of Custody : Present
Sample Tags : Absent
Sample Tag Numbers: Not Listed on Chain of Custody
SMO Forms : N/A
Sample Seals: Absent
Container...: Intact
TLI Project Number 42298
Client: ERG02 - Eastern Research Group
Date Received
+
07/01/97 By
Box
NO COOLANT
Carrier and Number | JIM GAUGHEY
60
IJTLI Number Client Sample ID Matrix | To LAB
jjmR/H-CPM Client COC ID * Location Date/Init
||I73-60-12D LTV-23 KMN04
IJ LTV-23 METALS LAB
II 1 1
||173-60-12E LTV-24 8N HC1 1
U LTV-24 METALS LAB j
|| 1 1
||173-60-13A LTV-26 NITRIC ACID|
|| LTV-26 METALS LAB j
II 1
||l73-60-13B LTV-27 HN03/H202)
|| LTV-27 METALS LAB j
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||173-60-13C LTV-28 0 . IN HN03|
jj LTV-28 METALS LAB |L- \
II J 1
JJ173-60-13D LTV-29 KMN04 j
y LTV-29 METALS LAB j
||173-60-13E LTV-30 8N HC1 1
y LTV-30 METALS LAB j
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||173-60-14A LTV-32 NITRIC ACID|
I) LTV-32 METALS LAB j
||173-60-14B LTV-33 HN03/H202J
|| LTV-33 METALS LAB j
yi73-60-14C LTV-34 0.1N HN03|
|| LTV-34 METALS LAB |.JA |
((173-60-14D LTV-3S KMN04 |
y LTV- 3 5 METALS LAB j
II I
yi73-60-14E LTV-36 8N HC1 1
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=Form Revised 05/27/1997 -- Page 4 OF 4
-------
ui.n, LJUjUKAlUKIfcb. INC. -- LOG IN RECORD/CHAIN OF CUSTODV=
|| Custody Seal : Absent Sample Seals: Absent
|| Chain of Custody : Present Container. . : Intact
|| Sample Tags : Absent
|| Sample Tag Numbers: Not Listed on Chain of Custody
(I SMO Forms : N/A
TLI Project Number 42434 Book ||
Client. ERG02 - Eastern Research Group 11
174 jj
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Date Received • | 07/14/97 | By f^/ ^/^7 Page ||
i i U7s^fsf/ />- ) n
II BOX NO COOLANT Carrier and Number | JIM M. /y ,^ 97 ||
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||TLI Number Client Sample ID Matrix | To LAB
jlmR/H-CPM Client COC ID . . * Location | Date/Init
II — i
|| 174 -97-1 2 ACETONE PROBE RINSE |
|| BEAKER *2 * METALS LAB j
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||l74-97-2 5 ACETONE PROBE RINSE)
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|| BEAKER #7 • METALS LAB j
||l74-97-8 8 ACETONE PROBE RINSE)
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|| LTV- 8 9 METALS LAB j
1)174-97-14 LTV- 92 FILTER]
|| LTV- 92 METALS LAB |
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-------
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|| 174 -97 -15 LTV- 90 FILTER
|j LTV- 90 METALS LAB
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||l74-97-16 LTV-93 FILTER
j| LTV-93 METALS LAB
|| 174 -97 -17 LTV- 99 FILTER
|| LTV- 99 METALS LAB
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||l74-97-18 LTV-39 FILTER
jj LTV-39 METALS LAB
Sl74-»7-l» LTV-8J FILTER
|| LTV- 52 METALS LAB
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||l74-97-20 LTV-46 FILTER
|| LTV-46 METALS LAB
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=Form Revised 05/27/1997 -- Page 2 OF 2=
-------
Project #
Client:
Date/lnt.:
ICP GFAA FLAA CVAA
Triangh
Client Runfl
(919)544-5729
fluUef>n
of RTP
cd',Co
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—
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redlssolve in _. . rl
10ml con HN03 Dale 4
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with cone. HF
nd cone. HNO3 Date
labe
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Int S/=
Reduce
volume
to 20 ml on „ .
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Volume 670
For Metals For h
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CONT # CONT «
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with cone. HF filiela W
and cone. HNO3 Date tjKO^y
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Reduce Volume Int. ^f~_
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Aliquot A: D ml
(No spike required)
Aliquot B:
Spike
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lnt
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, Volume jf^ylpate
Aliquot A: C <-i
Aliquot B:_J>Jri
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(One post digesllon spk on BH for GFAA)
D \2llcnmlior
-------
Project #_
Client:
ICP GFAA FLAA CVAA
Date/lnt.:
Triangle Laboratories of RTP
(919)544-5729
Client Run#
Volume /QD i
111
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Volume X?fQ
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10ml con HN03
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label
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with cone. HF
Microwave dig
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nd cone. HNO3
and cone. HNO3 Date
- 4
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and H202
label
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FH & BH Post dig. spk.
(Oio r>osl dlQesllon spk on 111 I (or GPAA)
ppb (instrument spiked)
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CONT «
| Hg Implngers |
CONT //
CONT
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ICP GFAA FLAA CVAA
Date/lnt.:.
Client
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(919)544-5729
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label
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Add
500 uL Sc
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Date
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Date:
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[ Hg Implngers
CONT «
©
KMNO4
CONTtt
© <
HC1 r'"
Volume Dry
Volume
Desslcate to •
dryness and
redissolve In ^ .
10ml con HN03 Date
label
label
Reduce
volume
to 20 ml on
For Metals For Hg
label label
i Aliquot A
j Aliquot
i i Aliquot A -^ : Aliquot;A_ ;5^_
j ! Aliquot B $ \ I Aliquot B_5
i i int «>^xi ; i int
Microwave dig
with cone. HF
nd cone. HNO3
Microwave dig Int
with cone. HF
and cone. HNO3 Date
(Duplicate Analysis of Each)
Combine dlgestates
Reduce Volume Int.
to 20 ml on
Hotplate
Spike
BH Hg Spike required)
Front Half Dlgestate
Hotplate dig
with HNO3
and H202
Dilute to
100 mis
Aliquot A:
Aliquot B:
Aliquot A:
Aliquot B:
; final spk cone. Date
'. addedppb
FH & BH Serial dilution performed
ml toml FV + uL Sc
10 ppst digest spike on FH (or GFAA))
(One r>ost digestion spk on Bl I lor GFAA)
FH & BH Post dig. spk.
@CD—_PPb (Instrument spiked)
Aliquot A: J^ ml
(No spike required)
Aliquol B: __h ml.
-------
ICP GFAA FLAA CVAA
Client:
Date/lnt.:
Client RunHMttfadffljIhk
COM/? com
Aceto
Rins«
Trinnnlp
1 1 1 V_>l 1 1 V— ^ 1 V~- '
^jF6l
« corjT#
1 ©
3ne - HNO3
" . Rin<;p>
Laboratories of RTP
(919)544-5729
COMT#
£* 0
Back Half
0^ Otf> CONT«
6^* \CP ^RA I
^* Afc ^- \\Ji\l
1 Hg Implngers
CONT «
(SB)
C
CONTfl
HC1
Volume_Dcy
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dryness and
redissolve in _ .
10ml con HN03 Date
label
Volume
Microwave dig
with cone. HF
nd cone. HNO3
label
Volume35/QsTi/
Reduce
volume
to 20 ml on
_ hotpjgt.e
1C
Microwave dig Int
with cone. HF
and cone. HNO3 Date
Combine dlgestates
label I73^0'5J) label
i Volume &S ml i; Volume ^75 ml i i Volume75 ml
Aliquot
Aliquot
0 S
j Aliquot
i Aliquot B_Zi£X. i j Aliquot R_-
ilnt iV\A- i i Int M<
Date
(Duplicate Analysis of Each)
Reduce Volume Int. oT—
to 20 mL on
Hotplate DateT
Front Half Dlgestate
Hotplate dig
with HNO3
and H202
Add
500 uL Sc
Volume /Ol) Ml'
Volume^
10 post dlQest spike on Fl I for GFAA))
Dale
spk on 011 for GFAA)
Aliquot A: Q ml
(No spike required)
I:H & BH Post dig. spk.
ppb (instrument spiked)
Sample
1
Spike
(1 BH Hg Spike requited)
i label
Int
!label!!?^6 mt
'Volume (00 pgte'folfo 1 iVolume Date
Aliquot A:J
Aliquot B:
Aliquot A:
Aliquot B:.
;spk
iof "
ml
I final spk cone.
; added ppb
Inl
Date
\?llmciilinrillVuMl\t;'>1
FH & BH Serial dilution performed
ml to ml FV + uL Sc
initials;
Date:
-------
Proiect# "VcPcQ^
Client:
Date/lnt.:
Client Run# MeUio
Analytes
gf ICP GFAA FLAA CVAA
Trianale Lnb^ratnri<^s <^f RTP
(9 19} 544-5729
T0c3kf.tf6a
/ /
CQN7#
C(SNL# COhJTtf COrJTtf
(c:9 C?y c (A) CONT#
Hg Implngers |
CONTS
^ -v
SONT#
V—*
Filter
:GorQ
Acetone
Rinse
label
HN03
label
Volume
Desslcate to
dryness and
redissolve in
10ml con HN03
Int
Date
Reduce
volume
to 20 ml on
hotplate
Int SF
Date "Hfr-'n
labeLLB^ -^f\ label H3- ^>O -6C
Volume ^5 Volume J15-'
>p-6rt /<
Volume /£n ml : Volume *K> ml
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label.
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: : Aliquot B
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Aliquot B
Int M^_
Microwave dig
with cone. HF
Microwave dig
with cone. HF
Date^/^A
and cone. HNO3 Date
and cone. HNO3
(Duplicate Analysis of Each)
Combine dlgestates
Reduce Volume Int. ^/^
to 20 ml on
Hotplate
Spike
(1 BH Hg Spike required)
Front Half Dlgestate
with
andH202
Dilute to
100 mis
Aliquot A:
Aliquot B:
Aliquot A:
Aliquot B:
label
volume
Dilute to
100 mis
final spk cone. Date
added ppb
^^v _^|Z i
te J1 fe W^olume-ml
FH & BH Serial dilution performed
ml to mlFV + uLSc
(One post digestion spk on BH for GFAA)
initials:
Date:
label
Volume
>ne post digest spike on FH for 6FAA))
FH & BH Post dig. spk.
ppb (instrument spiked)
(No spike required)
Aliquot B: __ST__mL
M 9 PP8O1 R \9tl
-------
project
Client:
i i/»v\ i
ICP GFAA FLAA CVAA
Date/lnt.:
Client
Triangle Laboratories of RTP
(919)544-5729
of RTP
•i
Filter
Type: G or Q
label
label
label
Volume
Int
Desslcate to
dryness and
redlssolve In ^ .
10ml con HN03 Date
T
Volume
Int
Reduce
volume
to 20 ml on ~ .
hotplate Date
: i
Hg Implngers |
CONTtf
CONT#
HN03
label
Volumei
i label
i Volume
ml
KMNO4 HCl
\ label I 'fcHQ-6^: label
: Volume oAaMnl ; ', Volume
ml
Microwave dig Int
with cone. HF
md cone. HNO3 Date
Microwave dip Int
with cone. HF
and cone. HNO3 Date
For Metals
label
ForHg
I
label
Aliquot A_
Aliquot B_
Int
i Aliquot A
i Aliquot
i Int
; Aliquot; A_
\ Aliquot B_
i Int _
Volume
Volume
Date
: Date
Date
Combine dlgestates
label
Front Half Dlgestate
t
(Duplicate Analysis of Each)
Reduce Volume Int. ,^nP
to 20 ml on
Hotplate Date"/-/?-*"
Add 500 uL Sc
i —
Dilute to
100 mis
Int
Date
i
For Metal
label
Volume
L
.ML
Hotplate dig
with HNO3
and H202
Int. OA
Datejjf
(P
^
i
Add A
SOOuLSc/ \
Int.
Date
Sample
I label
Int
I
Spike
(1 BH Hg Spike required)
label
Int
Volume
Date
; Volume
.Date
For Hg
label
Int
label
Int
Volume
Date
Volume ml Date
Aliquot A:.
Aliquot B:_
Aliquot A:
Aliquot B:.
; spk ml
3pb
Int
i final spk cone.
': added ppb
ie post digest spike on FH for GFAA))
FH & BH Post dig. spk.
@ — ppb (Instrument spiked)
CO
Aliquot A:
ml
(No spike required)
Aliquot B: ______ ml.
Volume Mi Date
(One post digestion spk on Bl I for GFAA)
M 2PCKVI U \2llmmliu r.
-------
Projects Hdd*
Client:
Date/lnt.:
Client Runff M^a
CONT#
0
Filter
Type: G or Q
%
Trie
1 1 1 V.
iMOaJ-ld^&l
CONT//
(5
1 Acetone
1 Rinse
Aiiuiyles
ICP GFAA FLAA CVAA
^ngle Laboratories of RTP
(919)544-5729
CONT//
(5
HNO3
Pinsp
^2
!£CJO
Back Half
1 Hg Impingers
U6« ,<0 CONT// CONT//
CONT //
©
tab^JlW-ao
label
Volume
Jky
Desslcate to
dryness and
redlssolve in ^ .
10ml con HN03 Date
Microwave dig
with cone. HF
•nd cone. HNO3
Reduce
volume
to 20 ml on „ .
hotplate Dale
(pO'HA label!'
Volume
te
label
Volume^?Q ml i : Volume /^ ml
Microwave dig Int
with cone. HF
and cone. HNO3 Date
Combine dlgestates
For Metals
I
label
ForHg
Aliquot A
I
label
Aliquot B
Int
_J>4- i i
i Aliquot A
Aliquot
i i Int
Aliquot; A
i Aliquot
\ Int
J^O VA3lume__ | DqteJ?|^fi] Mpate^h?
f ' ' — , (Duplica
Dote
Reduce Volume Int. SP
to 20 mL on
Hotplate Date
Front Half Dlgestate
Hotplate dig
with HNO3
and H202
Aliquot A:
Aliquot
Add
500 uL Sc
label
Volume
Dilute to
100 mis
post digest spike on FH for GFAA))
Volume /6Z> Date
Aliquot A: _ mL
(No spike requited)
Aliquot 0: _. £ ml
H&BH Post dig. spk.
ppb (instrument spiked)
(°ne P°sl dlgeslion spk on BH for GFAA)
(Duplicate Analysis of Each)
Spike
(1 BH Hg Splko required)
label
Int
; Volume
Date
Aliquot A:
Aliquot B:.
; spk ml
; of ppb
Int
I final spk cone. Date
j added ppb
FH & BH Serial dilution performed
ml to ml FV + uL Sc
inlllals:
-------
rrojeci
ICP GFAA FLAA CVAA
Client:
Date/lnt.:.
Client Run#
>n/
Triangle Laboratories of RTP
(919)544-5729
CONJ «
0
of RTP
Filter
Type: G or Q
Desslcate to . .
dr/ness and inT
redlssolve in
10ml con HN03 Date
Microwave dig Int
with cone. HF
nd cone. HNO3 Date
label 173 '(pO~l£A label
Volume /T)
Reduce
volume
to 20 ml on
to 20 ml on „ , —, KVG~»
hotplate Date >/r7Y
dconc^HNOa Datej?'
Combine digestates
CONTH
HNO3
Hg Implngers |
CONT «
SB
KMNO4
CONT
(sc)
MCI
i Volume 7T) ml i ; Volumec?/0 ml ; i Volume '70 ml i
• CT" ' ' s*~ : ^~ '
i Aliquot A/''? •
, added V ppb ' '—
label
; Volume.
(One post dlgeslion spk on Bl I for GFAA)"
51 II \7llinmlKirilr\iitliU; 91
FH & BH Serial dilution performed
ml to ml FV + nl. Se
Initials:
Dalo:
-------
Prelect # Vo/&C
Client:
Date/lnt.:
Client Run# /t^Of
©
3x7 Analytes
/£ ICP GFAA FLAA CVAA
Trinnolp> 1 rihorritpirip^ of PTP
III \~4 1 1 V-j 1 v^ \—\^\ t*J W 1 V_4 I ^J| I O O W 1 1 \ 1 1
r91 9^544-8799
1 cW.lnlef.Cun ^
/ /
CONT « COhJT # C04T «
(2) (3) (4) CONT#
| Hg Implngers
CONT «
CONT«
Filter
Type: G or Q
label I
label tf^-
Volume
Desslcate to lnt
dryness and lnt
redlssolve in _ .
10ml con HN03 Da'e
labelMl^- /2M Iabell^r6£~ ^
Volume SS Volume'
SA
HN03
SB
KMNO4
HC1
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volume
to 20 ml on
hotplate
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with cone. HF
ind cone. HNO3
Microwave dig
with
and
Combine digestates
label
Volume
Aliquot A
Aliquot B.
Inl
ml i ; Volume
i Aliquot A.
Aliquot
ilnt.
; Volume ^O ml
: Aliquot; A_
:- Aliquot B
i Int.
Front Half Dlgestate
(Duplicate Analysis of Each)
e post digest spike on FH for GFAA))
Reduce Volume Int. 5P
to 20 ml on
Hotplate Dale:Zr&<2l
Hotplate dig
with HNO3
and H202
Date
Add
500 uL i
Int.
Date
Sample
Spike
(1 BH Hg Spike required)
Int M/C
Date
Aliquot A:
Aliquot B:
j ilabe^-4.0-1 ^int_mg.
j |Volume(^*<- Date
Aliquot A:
l-"H & BH Post dig. spk.
-sj
@ JS^N ppb (instrument spiked)
Aliquot B:
1 spk ^ ml
i QffOO ppb
Int
I final spk cone. Date 7
-------
ICP GFAA FLAA CVAA
Client:
Date/lnt.:
Client
Triangle Laboratories of RTP
(919)544-5729
Filter
Type: G or Q
Volume Pry
Desslcate to
dryness and
redlssolve In
Int
I OUI«UIVtJ 111 ._
10ml con HN03 Date
CONTtf
Hg Implngers
CONTtt
CONT #
©
HNO3 KMNCM HC1
Reduce
volume
to 20 ml on n .
hotplate Date IZr
i Volume<5CLml i: Volume<£&)ml : '. Volume
^O
ml !
Microwave dig
with cone. HF
:nd cone. HNO3
For Metals For Hg
I '
label label.
i Aliquot
j Aliquot B.
i Int
i ; Aliquot A.
i I Aliquot B
;! Int
' Aliquot; A.
i Allquqt B.
i Int
r
°
Microwave dig Int
with cone. HF
Volume Jl2_ Date
and cone. HNO3 Date
(Duplicate Analysis of Each)
Combine digestates
Reduce Volume Int.
to 20 ml on
Holplale
Spike
(1 BH Hg Spike mqulied)
Front Half Dlgestare
Hotplate dig
with HNO3
and H202
Aliquot A:
Aliquot B:
Aliquot A:
Aliquot B:
Volume |/T6 Ml '
lnt_Jfc(L_
Date •7Ji>/'i>7 i
H — ' —
final
added
FH & BH Serial dilution performed
ml toml FV + uL Sc
A,, . A
-------
PAGE
INORGANICS SPIKE LOG
DATE
PROJECT *
SAMPLE IDs
ANALYTE
ORIGINAL
STANDARD
ORIGINAL
STANDARD
CONC.
(PPM)
SPIKE
SAMPLE
FINAL
VOLUME
(mL)
SPIKE
SAMPLE
(PP9)
INITIALS
WITNESS
QQ
5F
3S
*
175-1 -
1
UZL
IMS
MSO
/
4f
S
qa\forms\inospke.log (08/22/96)
74
-------
JLl
* SEE SPIKE LOG
• Spiking Standard
Element Standard Ong. Std.
ID (ppm)
*g
*s
ia
>tf
»b
5b
>« .
n
n
/
in
Zn
2-115^
2-115-3
-2-115-4
2-1 05-7
2-115^4
2-115-4
2-115-3
2-115-3
2-1 05-8
2-115-3
2-115-3
2-115-3
2-115-3
2-115-3
2-1 05-9
2-115-4
2-1 08-7
2-115-3
2-1 06-1
2-115-3
2-115-3
2-115-4
2-1 08-6
2-115-3.
2-115-3
, 2-115-3
..2-t15-3
2-115-3
2-115-3
2-115-3
2-115-3
2-1 06-5
100
100
100
10000
100
100
100
100
10000
*100
100
100-.
100
100
10000
1000
10000
100
10000
- 100
100
100
10000
r-too
-100
.-100
-100-
100
100
100
100
1000
Preparation
Spika(uL) cone
Fvol(IOOmL)
5000
5000
5000
950
5000
5000
5000
5000
950
••- 5000 -
5000
• 5000- --U
5000
5000
950
5000
1500
5000
950
'• 5000'"
3000
5000
1950
; T5000 - ~
:: sooo
v 3000"*
... -500O
5000
5000
5000
5000
1500
(ppm)
5
•"* '-
5
'5
3
5
5 -
5
95
5- *,
4- 5 -*
, w.s5 -
5
5
95
50
150
5
95
- ..-5 :-,,-
5
5
195
...:.•' 5 -
. -^5 _
»-»«v-5r-
-,-. 5— **
5
5
5
- 5
15
SPIKING
lrom Spiking Standard
Spike(uL) cone
=Vol(100mt)
1000
....1000
1000
1000
1000
1000
.. .1000 •*•
1000
1000
iooc«*:
— 1000-4
.1000 .«
1000
1000
1000
1000
1000
1000
1000
"3-1000U"
1000
1000
1000
~tOOO- i-
•100O-">
1000"-*.
vKtOOO- •
1000
1000
10OO
1000
1000
(ppb)
50
-.--so *
50
950
• ^—i
50 '
-'«5O.W
bU ,
950
-^550,^
.-•csoirv
«,;5o:a«
50
50
950
500
1500
50
950
"^•50 -<
50
50
1950
»-t-5O:«_
*>*50 v
^*»5O -*
— 50 -»
50
50
50
50
150
combined
total
,1000
1000
1000
2000
1000
2000
200
QQQuL of tne Spiking Standard gives the listed cone, ot tne afiove elements.
"Spike separately
Element Orig Std Spike(uL) cone
(ppm) Fvoi(100 (ppb)
Au
Ce
Li
P
Pd •
Pt
S
Si
Sn
Sr
1000
1000
1000
1000
1000
1000
1000
10000
1000
1000
140
30
70
100
160
300
350
350
20
5
1400
300
700
1000 .
1600
3000
3500
35000
200
50
Spiking Standard 3-001-8
EXP: 8/31/97
Spiked by:
Predigestion-
Postdigestion-
75
-------
PAGE 1 OF 3
f _________ _ _____ _ _ _ _ _ _ — ,
TRIANGLE LABORATORIES, INC.
Transfer Chain-of-Custody Form
Project
42298
Transfer From: IWLM To: IA I
Released by:
Accepted by:
MILES. ID
42298- -000
42298- -001
42298- -002
42298- -003
42298- -004
42298- -005
42298- -006
42298- -007
42298- -008
42298- -009
42298- -010
42298- -Oil
42298- -012
42298- -013
42298- -014
42298- -015
42298- -016
42298- -017
42298- -018
42298- -019
42298- -020
42298- -021
42298- -022
42298- -023
42298- -024
42298- -025
42298- -026
42298- -027
42298- -028
42298- -029
Initials . .
rt&r
TLI No
TLI Blank
173-60-1A
173-60-1B
173-60-1C
173-60-1D
173-60-1E
174-97-1
173-60-10
174-97-11
173-60-2A
173-60-2B
173-60-2C
173-60-2D
173-60-2E
174-97-4
174-97-13
173-60-3A
173-60-3B
173-60-3C
173-60-3D
173-60-3E
174-97-6
174-97-15
173-60-4A
173-60-4B
173-60-4C
173-60-4D
173-60-4E
174-97-8
174-97-18
Date Time
JL/.32/-22 l6-.3of>*<
Cust .Id. ...
TLI Method Blank
LTV- 02
LTV- 03
LTV- 04
LTV- 05
LTV- 06
2 (=LTV01)
LTV- 101
LTV- 8 8
LTV- 08
LTV- 09
LTV-10
LTV- 11
LTV- 12
3 (=LTV07)
LTV- 8 9
LTV- 14
LTV-15
LTV- 16
LTV- 17
LTV- 18
4 (=LTV13)
LTV-90
LTV- 3 8
LTV- 40
LTV- 41
LTV- 4 2
LTV- 4 3
8 (=LTV37)
LTV- 3 9
Additional comments or instructions:
76
-------
PAGE 2 OF 3
TRIANGLE LABORATORIES, INC.
Transfer Chain-of -Custody Form
Project
42298
Transfer From: IWLM To: IA I
Tn i t~ i aT
-------
SEP-17-97 WED 05:53 PM TRIANGLE LABS
FAX HO, 919+544+5491
P.02
PAGE 3 OF 3
TRIANGLE LABORATORIES, INC.
Transfer Chain-of-Custody Form
Project 42298
Transfer From: IWLM To: IA I
Initials.. Date
Released by: Q)l^ \J_
Accepted by:
Time,
MILES.ID.
42298-
42298-
42258-
42298-
42298-
42298-
42298-
42298-
42293-
42298-
42298-
-060
-061
-062
-063
-064
-065
-067
-068
-069
-070
-071
TLI No,
173-
173-
173-
173-
173-
173-
173-
173-
174-
174-
LCS
60-SC
•60-6D
•60-6S
50-7
•SO-11A
SO-11B
60-liD
60-11E
97-10
97-20
t.Id.
LTV-60
LTV-61
LTV-62
LTV-57
LTV-45
LTV-47
LTV-48
LTV-49
9 (=LTV44)
LTV-46
Lab Control Spike
Ackiitio:ial comments or instructions
-XfrCOC (Rev n/01/94)---
78
-------
-------
* SEE SPIKE LOG
Spiking Standard Preparation
Element Standard Ong. Std. Spike(uL) cone
ID (ppm)
*g
As
41
Al
3
3a
3e
~a
Za
:d
So
:r
:u
:e
:e
<
(
tfg
dg
vln
vlo
•Ja
•Ja
Ji
>b
Sb
3e
T
n
^
Zn
Zn
2-115-4
2-115-3
2-115-1
2-1 05-7
2-115-4
2-115-4
2-115-3
2-115-3
2-1 05-8
2-115-3
2-115-3
2-115-3
2-115-3
2-115-3
2-105-9
2-115-1
2-1 08-7
2-115-3
2-106-1
2-115-3
2-115-3
2-115-4
2-108-6
2-115-3
2-115-3
2-115-3
2-115-3
2-115-3
2-115-3
2-115-3
2-115-3
100
100
100
10000
100
100
100
100
10000
100
100
100
100
100
10000
1000
10000
100
10000
100
100
100
10000
100
100
100
100
100
100
100
100
Fvoi(IOOmL)
5000
5000
5000
950
5000
5000
5000
5000
950
5000
5000
5000
5000
5000
950
5000
1500
5000
950
5000
5000
5000
1950
5000
5000
5000
5000
5000
5000
5000
5000
2-106-5 i 1000 | 1500
(ppm)
5
5
5
95
5
5
5
5
95
5
5
5
5
5
95
50 |
150
5 I
95 I
5
5
5 I
195
5 !
5 I
5
5
5
5
5
5 I
15
SPIKING
'rom Spiking Standard
Spike(uL) cone combined
=Vol(100ml)
1000
1000
1000
1000
1000
1000
1000
1000
1000
1000
1000
1000
1000
1000
1000
1000
1000
1000
1000
1000
1000
1000
1000
1000
1000
1000
1000
1000
1000
1000
1000
1000
(ppb) total
50
50
50
950
50
50
50
50
950
50
50
50
50
50
950
500
1500
50
950
50
50
50
1950
50
50
50
50
50
50
50
50
150
1000
1000
1000
2000
1000
2000
200
"Spike separately
Element Orig Std Spike(uL) cone
(ppm) Fvol(100 (ppb)
Au
Ce
Li
P
Pd
Pt
S
Si
Sn
Sr
1000
1000
1000
1000
1000
1000
1000
10000
1000
1000
140
30
70
100
160
300
350
350
20
5
1400
300
700
1000
1600
3000
3500
35000
200
50
10OOuL of the SpiKing Standard gives tne listed cone, of the above elements.
Spiking Standard 3-001-9
EXP: 8/31/97
Spiked by:
Predigestion-
Postdigestion-
80
-------
sis Reoor;
Summary
(Ion OX5-37 07:04:58 AM
oaoe 1
It Samole Kane
File
Metnod Date
Time OoID Type Mode
1 STOl-BLANK
2 STD3
3 STD3
4 CHECK LO
5 ICV/CCV
7 IC8/CC8
8 ICSAB
.
.AA/V
yYV^v
~k
f\
81
-------
Analysis Reoort Sundry non 07-28—7 07:04:58 AM cage 2
It Sanple Name File Method Date Tiae OcIO Tyoe Moae
54
55
56
58-
59
60
173-60-14A X10 7279
173-60-18 7279
ICV/CCV 7279
ICBTttB 7279
1C8/CC8 7279
ICSA8 7279"
/ TRIANGL2
7 TRIANGL2
1 TRIANGL2
f ' IKIHNbLZ
7 TRIANGL2
f TRIANGL2
07/28/97
07/28/97
07/28/97
"0//2H/9T
07/28/97
07/28/97
06:
06
06:
"U51
06:
06:
13
19
24
75"
40
45
OXH
DKH
DKH
TJKH
DKH
DKH
S
S
0
0
0
0
CONC
CONC
CONC
cotte
CONC
CONC
82
-------
PAGE 1 OF 6
TRIANGLE LABORATORIES, INC. 1
Sample Preparation Tracking & Management Form I
ece. 42298 Client: Eastern Research Group (ERG02) I
Sample Information j r 1
•thod- T /Cx Extraction Date: / / \ \ ^1 '
,lvenC/Acids ( ) : -H A/*?} lHLl&f, Lot : " 7 S LC / 1, fe 0fO / |
1 1 1
| TLI / 1 Sample |Fina
iple| SAMPLE ID / CLIENT |Wgt //Vo"l|Volu
crd| / SAMPLE ID | g /W | ml
i ^^ i i i - 1 i i
i i aijcvfec^i i i I I i
me|//|//l//l//l//l//l
1 1 1 1 1 1 1
| TLI Blank I ,! ft 1 , R 1 1 1 1 1 1 1
| N/ftT) TLI Method Blank | N 1 /T | I ^U | | | | I 1 1
1 m cn-uv. . 7/1?'*' /ve— 1 1
| LTV-02 | |
| 173-60-1B 1 J jr \
1 •-) \ LTV- 03 | .Xff; \
\ 173-60-1C 1 ^/* 1
| 173-60-1D 1 ~>/' \
| 173-60-1E 1 C.. s'\
1 l")\ L ' N LTV-06 | /( \
\ 174 37 1 7/t-f/l? '*- 1 I
| 2 (-LTV01) | |
1 1 1 1 1 1 1
1 1 1 1 1 1 1
1-1,1 1 1 1 1 ' 1
1 '|ZV7l 1 1 1 1 1
1 7/7, /«n 1 1 1 1 1 I
i 'I2- < v i i i i i i
1,1 1 1 1 1 !
i 7 "^n? i i i i i i
1 / 1 ! I 1 1 1
1 7/^/97 1 1 1 1 II
1 1 1 I 1 1 1
1 1 1 1 1 1 1
| LTV-101 III 1 1 1 1 1 1
[ 174-97-«r l//f | ^S 1
1 ,-v c-» //, -^ LTV-88 \ / £ \
1 (TH-^T" y/f ^ X ^
| LTV-08 | |
| 173-60-2B 1 5x> 1
1 t7^"bo-2 0 l\ LTV-09 \ /*•) \
I-,/ , 1 1 1 1 1 1
i '/^/V i I - I I I I
1 1 1 1 1 I I
1 I 1 1 1 I 1
!7H*7| ! ! ! ! !
\ 173-60-2C 1 ^}/' ' I ' -7 j IG ' ' ' ' ' '
| ,->, / - . -j ^ LTV-10 | /S || / ' / ^ 1 1 1 1 1 1
| 173-60-2D 1 S/p 1 I/ 1 7/1,1 1 ' ' ' ' ' '
+ + + + H + " * » »
|
ment3: ^e.t HGSL-I p. S'S $*}
-------
PAGE 2 OF S
* -f
TRIANGLE LABORATORIES, INC. |
Sample Preparation Tracking & Management Form |
i Project: 42298 Client: Eastern Research Group (ERG02) |
"")( f *~7 O Sample Information . |
Method: '\ ' Extraction Date: / / /7CT 1
Solvent/Acids 0 : HAJO. / R,iO.X Lot: l'?0 2.° / J/(? 0£"O ' "/ |
/ ' '
1 III ^fe . 1 1 1 1 1
| TLI / | Sample [Final | ^3^^- | 1 1 1 1
Sample 1 SAMPLE ID / CLIENT |Wgt / WolN Volume 1 //I// //I//I//I//I
# crd | / SAMPLE ID | g / tnl \ ml | | | | | |
1 173-60-2E | VX I/QQ | I | | | | |
013 ipi-ko-2-t LTV'12 '/s i i '!Lin7 1 i i i i
| 174-97-4 7^3 1 J./^- 1
014 i j?u_ G7_ U. lj-> ;\ 3 (-LTV07) Ix/b 1
015 | LTV-89 | |
-,Kr/t7^Z.
1 17J.iO"3A-'- '/ <" \ \
016 | LTV- 14 | |
| 173-SO-3B | ~>/^ 1
| 173-60-3C | JX* 1
318 | n3-feo-,Jc ?\ LTV-16 | -/X"' |
| 173-60-3D | S/^l
319 | nS-lp^-JN LTV-17 1 -XtT 1
| 173-60-3E | ^" .X' |
320 | (7- t^_^r LTV-18 | x^V" |
1)21 I n^-Si-fe/^s' _^ 4 <-LTV13) |/<^ '
|-t^i.a7-i5 -?li-t/f>i^t- 1 I
322 | LTV- 90 | |
| 173-60-4A Pj | Sx^" '
323 1 i-)J- feo-v^^ ^, X LTV-38 I/V' 1
(—• WT'Off'+B 't'Tft? ^" 1 1
)24 | LTV-40 | |
| 173-SO-4C | S^^^ 1
125 | p3-y>0-L(£_ ^ LTV-41 _^/^^ 1 y
1 , . 1 1 1 1 1
i7W; i i i i i
ii i i i i
i i i i i i i
i i i i i i i
i i i i i i i
i,i i i i i i
1 "7(1^7 1 1 1 1 1 1
I-/.I 1 1 1 1 1
1 "1T1 \ \ 1 - I I I
I , I I I I I I
I7'V7V i i i i i i
i , , i i i i i i
i7!7-1^ 7 i i i i i i
!?MV! : .; : : ;
1 1 1 1 I ! 1
1 1 1 1 1 I 1
1 i , 1 1 1 1 ! 1
i 'll
-------
PAGE 3 OF 6
TRIANGLE LABORATORIES, INC. I
Sample Preparation Tracking 4 Management Form I
onecc- 42298 Client: Eastern Research Group (ERG02) |
Sample Information I
thod- ' M 1 Extraction Date: / / -J-'/ g. 1
Ivent/AcidsO: MO, /KL$CJ. Lot: ||7DiO /3^0?O |V~") |
*l + ._L___ :W. ,
i i i
| TLI / 1 Sample-,. |Fii
ple| SAMPLE ID / CLIENT |Wgt /AtoI|Vo
crd| / SAMPLE ID | g /($/ \ '
»i i i i i i i i
Lumel //I//I//I//1//I//I
nl 1 I 1 1 1 1 1
| 173-SO-4D 1 ^s* '/P\O 'T/TC/C ' ' ' ' ' '
| 173-60-48 DC. 1 *J./'\
1 nj-to-Hj)^- £> LTV"43 '/i '
| 174-97-8 //^ 1 $/*''
1. Q / T 'nr^ "7 } 1 .^^f \
IT^I £ 7 C-/ /Cx A " t»Lil vj / / | S^ L \
\ LTV-39 | I
| 173-60-5A 6 1 S/' 1
1 \7i-fc c-fA-ft ^ LTV-51 1X5 1
t • J " *^ / -^
|"133 OO'SS •>/"/»""<_ | |
| LTV-53 | I
| 173-60-5C 1 ^^ 1
' 173 feO 5"C ft LTV-54 \/^~) 1
| 173-SO-5D 1 ^/^ 1
1 ni-bo-56 ii LTV-55 '•/^T '
| 173-60-5^ f>Q, 1 C .X" 1
'oj-w-s-oe- £> LTV'56 'XS '
| 174-97-9/ /"^ | C/ 1
' 1 7U. / N 10 ("LTV50) l/^^ '
| LTV-52 | |
| i?3 -fro- 12A I)1*/*'' "*- \ \
\ LTV-20 | |
| 173-60-12B 1 3?Xx'' '
i nj-to-aft £ LTV-21 IX) '
!_./,! 1 1 1 1 1
i fl^n? i i i i i i
+ , + _.+. + + -+
1 -/ , 1 1 1 1 1 1
1 7|M[17 | | | | | |
1 1 1 1 I ! 1
1 1 1 1 1 1 1
l-y f 1 1 1 1 i 1
I/Mr? i i i i i i
i i i i i i i
i i i i i i i
i , i i i i i i
/ / i i i i >
i"7'11/'*? i i i i i i
i i i i i i i
i i i.i i i i
i -i , i i i i i i
1 7/7?/V, 1 1 1 1 !
i i i i i i i
i i i i i i i
i i i i i i i
i i i i i i i
i '/ / ' i i i i i i
\\f \ i i i i i i
^ p- 1 !
i
i
-REV 07/26/93 (PSTMF 7)--+
85
-------
PAGE 4 OF S
TRIANGLE LABORATORIES, INC. j
Sample Preparation Tracking & Management Form |
Project: 42298 Client: Eastern Research Group (ERG02) |
•"7U-7O Sanple Information I |
Method: ' ' Extraction Date: / / 1 ' ^ 1
Solvent/Acids 0 : -H^* /ni.$0«*- Lot: i\~> OLO Mf40j"O / 1
• / T I ^
\ 1 1
| TLI / | Sample^Fii
Sample! SAMPLE ID / CLIENT |Hgt / iVol/Vol
# crdf / SAMPLE ID | g / Ul/| IT
1 cfWtt 1 1 1 1 1 1
«1 1 ' 1 1 1 1 1 1
u»e| / ... / 1 / / 1 / / 1 / / I / / I / / 1
1 1 1 1 1 1 1 1
1 173-60-12C | 5/ '/nO'v/T lit I 1 1 1 1 1
039 'nj-kO-lLCj) LTV-22 l/^- \[\J^\'\ 'H7 | | | | 1 |
| 173-60-12D | S/ 1
040 | i-7i.bO-lZli N LTV-23 \ S*Z. '
| 173-60-12E | ^s* I
041 1 HVU-IZC LTV-24 \ /£ \
\ 174-97-2/3 | £-, \
042 l(7U.cy7_7/? \ 5 <-LTV19> I /^ I
043 | LTV-91 | |
044 | LTV-26 | |
| 173-60-13B | ta/r 1
545 Inv-Lo-Krt LTV-27 \/ (~ \
\ 173-60-13C | ^l/^' 1
346 'Hi- bO- IU b LTV'28 'XS '
| 173-60-13D I ^S^ '
547 l|7l-V,O-llfi tN LTV-29 \ /f \
\ 173-60-13E I Cy^ \
348 ' O L 1 - (\ LTV-30 LXV' 1
349 | .,^ --/ 6 (-LTV25) | /£ \
|~-3r74-97-l«- it'''/''' •*• | I
J50 | LTV- 92 | |
1 1 7 1 - fi fl - 14ft 7 /i W*» 7 *^"^ 1 1
351 | LTV-32 | |
1 | i 1 1 1 1 1 1
pp'r*? i i i i i i
i / , i i i i i i
i v2-'/9? i i i i i i
i / i i i i i i
i i i i i i i
i i i i i i i
i i i i i i i
i i i i i i i
i.i i i i i i
i T2-'/''? i i i i i i
i _/ 1 i i i i i i
i 'r'n7 i i i i i i
1 , , 1 ! ! 1 1 1
pp-'p? 1 1 1 1 1 1
1,1 1 1 1 1 1
Pp-'/v i i i i i i
1 i 1 1 1 ! 1 1
i/rW i i i i i i
i i i i i i i
i i i i i i i
ki i i i i i i
i i i i i i i
^r P 1 !
Comments : o>-c. \ ' 1 1
1
1
-REV 07/26/93 (PSTMF 7)--+
86
-------
PAGE 5 OF 6
TRIANGLE LABORATORIES, INC.
Sample Preparation Tracking & Management Form
Project: 42298 Client: Eastern Research Group (ERG02)
Method: ' T ' Extraction Date:
Solvent/Acids 0: \-1 fJ^ \ 1 P* L& & Lot: Hl^iOi
Sample Information
,-'-'- fk
'i/feCKJ . 1
lit -«
1 1 1 '^P" 1 1 1 1 1
1 TLI / I Sample (Final | ^J*/^ 1 1 1 1 I
uitDlel SAMPLE ID / CLIENT (Wort //Vol (Volume 1 //I//I//I//I//I//J
crd| / SAMPLE ID | g /I nd/ | ml | | | | | | [
| 173-60-14B I fT^. 'fOO' -)l 1 ' ' ' ' ' '
32 i 173-40 -/^6 .£> LTv-33 i/f^ ' ' l^n? i i i i ! f
| 173-60-14C | £1 ^f^
53 'nj-to-iifc 3 LTV'34 ' /\ '
| 173-60-14D | C.X 1
54 1 HI (0/UM\ LTV-3S | ,/T |
| 173-60-14E | J/^l
55 l|"7t.Ll,/ur LTV-36 | /T \
\ 174-97-7 J/lc | C' |
>S 1 / x 7 (-LTV33) 1 ST \
n^-^l- 7//6 0 / S
i7 | LTV-93 | |
| 173-60-6A H.J 1 ^y^S* 1
>8 1 L, n -H LTV-58 | .sC 1
| 173-60-6B | ^/* 1
59 1 1 7i-t?O-k£ j) LTV-59 | ./X |
*<^li? ^t- --
| 173-60-S^ <^ C- i L>S^\
| 173-SO-6D | ^/^" 1
il Ini-tO-tb 5 LTV-61 l/^ 1
| 173-60-6^ ^ Q. | ^ S* |
52 1 1-,, , ^ /• v LTV-62 | >XT |
1 Oi-to -C.be l> / J
| 173-60-7 | S/^ 1
i3 | pj-feo-'' t> LTV-57 \/C 1
| 173-SO-11A 5 1 ~? >X |
'4 1 Oi- ^ LTV-4S \j'C) |
'-? ^||L / 1 1 1 1 1 I
I W*7 i i i i i i
'"M i i i i i
i-j , i i i i i .
17/11/17' i i i i f
/i ' ' 'i i i i t t
f
Vpe « |
romments : 0^*- r * ! • 1"
t
i
-REV 07/26/93 (PSTMF 7)--+
87
-------
PAGE 6 OF 6
Project: 42298
TRIANGLE LABORATORIES, INC.
Sample Preparation Tracking & Management Form
Client: Eastern Research Group (ERG02)
Method:
Solvent/Acids ():
,
Sample Information
Extraction Date: / /
Lot: lf70Z.O /I,(,0i0
| TLI / | Sample |Final | K .• \ \ \ \ \
Sample I SAMPLE ID / CLIENT |Wgt //Vofy Volume I /V Y^ I//I//I// //I//I
# crd| / SAMPLE ID | g A ml l\ nl | | | | | |
tG~
'•i^t-to^Tffrib' £> LTV"4? ' '
| 173-60-11D | S/^ |
067 | m-(,o-|f,£ i\ LTV-48 1 Xx" \
j 173-60-11$ !>£- | ^.S \
\ 174-97-10 J1O 1 J/* 1
069 | i-jujc nl \ 9 (-LTV44' 1 /dC
070 | LTV-46 | |
1 T rc 1 i 1
A/ A-
071 1 / f i t~> k**3 Control Spike | '^ If' |
|H3-feo-^/V I C/'l
| |7j-fco- /f ftj> L/b '
Tl Til
1 t-'TS •• V&- - ir*i('i7 i i
1 TV2.. 1 1
1 1 1
oi4'/*/~i ii ii
i T?/2-V''7 111 ii
1 '"'?? III II
1 , , 1 1 1 1 1
iWv 111 ii
1 7/^ III II
1 ' "' 1 1 1 1 1 1
1 1 1 1 1 1 1
1 1 1 1 1 1 1
1 1 1 1 1 1 1
1 1 1 1 i 1 1
1 / / 1 1 1 1 1 1
1 'I2™? 1 1 1 1 1 1
1 1 1 1 1 1 1
1 1 1 1 1 1 1
^i- 60 -11- ft MJ 1 ^/ 1 |7^? 1 1 1 1 1 1
I (7y bo- i ^ 5 M s jv> i/^ ' ' ' ' ' ' '
tPS- Wo - li'l i^J I c/. | | -,, , | | | | I I
mi'Uc- \\$ i-vs£ i x/ ^ ' ' i i i i i i
.P3-ICO- \W KS 1 rX 1 1 / f 1 1 1 1 1 1
-tX*^ *^1 (^ 1 Q "^
im-U- 1H(5 i^S C> 'x^^ ' ' ' ' ' ' ' '
,h3- to-lS M5 | <^| Inf^/,, 1 1 1 1 1 1
i nj-to -Ift MJ (^ >x^V ' ' 7 ' ' ' ' ' '
1 113-^0 - ts ^5 | 5^^, l-7|tc/«7 I 1 1 1 I I
l<7i-feo--L(b f^sji I/^S 1 1 ' '''/ 1 1 1 1 t 1
S^^ h / '
Comments : OCx^ P • | 1
1 1
1
-REV 07/26/93 (PSTMF 7)--+
88
-------
PAGE 1 OF 1
reject: 42298
TRIANGLE LABORATORIES, INC.
Sample Preparation Tracking & Management Form
Client: Eastern Research Group (ERG02)
. TV 70
ethod:
olvent /Acids 0 :
Sample Information
Extraction Date: _ / _ / _
Lot: )(7Qt-Q
I TLI /
mple| SAMPLE ID / CLIENT
crd| / SAMPLE ID
I I I ^rc- I
I Sample (Final | dijttkj j
| Wgt / /Vci | Volume | / / | / /
| g /Iml l| ml | |
' !__/__/ I / / I / / ! / / I
| TLI Blank
I
I
I
TLI Method Blank
yf7j-~co~"3~s
1 nj- to -^ &
-to-
-REV 07/26/93 (PSTMF 7)--*
89
-------
PAGE 1 OF 1
rject: 42298
TRIANGLE LABORATORIES, INC.
Sample Preparation Tracking & Management Form
Client: Eastern Research Group (ERG02)
Method: /H /U
Solvent/Acids 0 : fo *^*i /•Hj^t
Saniple Information
Extraction Date: / /
i f 1 — * /
Lot:
rl
3
| TLI /
Sample! SAMPLE ID / CLIENT
# crd| / SAMPLE ID
| •"•H7 i'1'T'i i i i
I Sample -jFi=al I I I I
|Wgt //VoJ|Volume| / / | / / | / / | / /.
| g /{ml/1 ml |
| 173-SO-SA
058 |,
1
LTV-58
I
.
1 LC.S
i
1 1
I
-REV 07/2S/93 (PSTMF 7)-- +
90
-------
MERCURY SPIKE LOG
PAGE
DATE
PROJECT #
SAMPLE IDs
ORIGINAL
SPIKE
CONC. (Hg)
STANDARD #
WORKING
STANDARD
FROM
SPIKE
AMOUNT
(mL)
SPIKE
SAMPLE
(PPB)
INITIALS
WITNESS
_MiEL
H3- n-70
m-IVlD
\i
V
\L
L
7/f7/?7
0-l
ff*
3-
-------
PAGE
MERCURY SPIKE LOG
DATE
PROJECT #
SAMPLE IDs
ORIGINAL
SPIKE
CONC. (Hg)
STANDARD #
WORKING
STANDARD
PREPARED
FROM
SPIKE
AMOUNT
(mL)
SPIKE
SAMPLE
(PP8)
INITIALS
WITNESS
7-21-97
3-OO1
-7-Z- 2. fns i]
±
i
i
I
.2
O-
3-oof-t
175-
.vf 0-
-^
^^7
W52t
0'
1 -OoS-g-
MS
- IMGc
iL
vr
3-007-4
16
-?3-'pO-"2-S
7i-fer>- Zft
in- bo -
7^~c''7: f^fr
MJ
^3-bO-fcQ^
i.
qa\forms\hgspke.log (08/22/96)
92
-------
PAGE
MERCURY SPIKE LOG
DATE
7-JW
*
;-
PROJECT #
SAMPLE IDs^^
MwZlffi*
l~?3- &C-GA- ny
/73~ to- 6^Ms.^
ORIGINAL
SPIKE
CONC. (Hg)
0- \ff*~
I
•
STANDARD #
WORKING
STANDARD
PREPARED
PROM
^-007-6
vl/
.
•
-
SPIKE
AMOUNT
(mL)
5"^
J/
SPIKE
SAMPLE
(PPB)
5f(S,
I
INITIALS
/Hxf.
^
WITNESS
>^
\l^
qa\forms\hgspke.log (08/22/96)
93
-------
n)
3 Saiole (16(ii!)
4 Saiple (16n)
5 Saaole (16u)
— Sasole Sets —
Setl Type Prepare?
Usage
STO/GC/8LANK
Saioles
Saiples
Saioles
Saiples
Description
IPos Left
13
19
48
48
48
Method
Analyses/Pos
10
1
1
1
1
IPos Rack} StartPos
1 Norial No 42298
— Preparation Info —
Set* Uotake Uotakei2 Final Oil.Factor
G)
flk*
No Samples Preoared.
Rack
Pos
1
2
3
4
5
6
(7..
Rack
Pos
1
2
3
4
5
6
7
8
9
10
11
12
13
14
15
*1
RON
1
1
1
1
1
1
.19
»2
RON
1
1
1
1
1
1
1
1
1
1
1
1
2
2
2
Col
1
2
3
4
5
6
Not
Col
1
2
3
4
5
6
7
8
9
10
11
12
1
2
3
Saiole Name
STD3
STD1-BLANK
ICSAB
CHECK LO
ICV./CCV
IC8/CCB
Used)
Sanple Naie
42298 m
42298 LCS
173-60-1A.10
173-60-1A.10 POS
173-60-1A.10 L
173-60-2A
173-60-2A OA
173-60-3A
173-60-4A
173-60-5A
173-60-6A
173-60-11A
173-60-12A
173-60-13A
173-60-14A
Set t
-HA-
-HA-
-HA-
-HA-
-HA-
-NA-
Set t
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
tUsed
2
1
2
1
4
4
tUsed
-HA-
-NA-
-NA-
-HA-
-NA-
-HA-
-NA-
-HA-
-NA-
-NA-
-HA-
-NA-
-HA-
-NA-
-HA-
Type
Standard |~ '
Standard
DC Standard 1
DC Standard
OC Standard v
QC Standard
Type
Saiple
Saiple
Saiple 5n
Saiple ^
Saiple
Saiple
Saiole
Saiple
Saiple
Saiole
Saiole
Saiole
Saiole
Saiole
Saiole
94
-------
AutoSanpler Reoor: Table: HA412
Rack »2
Pos Ron Col Saiole Nane
Non 07-28-97 00:53:33 AM page 2
Set I fused Type
16
17
18
19
20
21
22
23
24
25
26
27
28
29
(30.
Rack
Pos
(1..
Rack
Pos
u..
Rack
Pos
(1..
2 4 173-60-18
2 5 173-60-18 POS
2 6 173-60-18 L
2 7 173-60-28
2 3 173-60-28 DA
2 9 173-60-38
2 10 173-60-48, 4A
2 11 173-60-58. 5A
2 12 173-60-6A.6C
3 1 173-60-7
3 2 173-60-11A,116
3 3 173-60-128
3 4 173-60-138
3 5 173-60-148
..48 Hot Used)
13
RON Col Saiple Nane
.48 Not Used)
14
Row Col Saiple Naie
.48 Not Used)
J5
RON Col Saiole Naie
.48 Not Usea)
1
1
1
1
1
1
1
1
1
1
1
1
1
1
Set 1
Set »
Set t
-MA-
-NA-
-NA-
-NA-
-NA-
-NA-
-NA-
-HA-
-HA-
-NA-
-NA-
-NA-
-NA-
-NA-
tUsed
fUsed
lU'sed
Saiole i
Saiole ^,
Saiple
Saiole
Saiole
Saiple
Saiple
Saiple
Saiple
Saiple
Saiple
Saiple
Saiple
Saiple
Type
Type
Type
JU^'i\kt4uxA "Vv
95
-------
Analysis Reoort
Averages
rton 07-28-97 06:51:53 AM oaae 1
Methoa: TRIANGL2 Samole Name: STD1-3LANK Ooerator:
Run Tine: 07/28/97 01:24 Fiienase: 72797
Mode: IR Tyoe: X Corr. Factor: 1.00000
Lab 10.: Cust. Siol. ID.: Cust. 10.:
Eleis Ag3280 A13082 Asl890 8_2496 Ba4934 8e3130
Units count count count count count count
Avge -.00003 .00454 -.00026 .00429 .00056 .0004
SOev .00077 .00002 .00007 .0002 .00002 0
*RSD 2024.96 .6375 26.3763 4.80011 4.69196 1.86591
Eleas Ca3179 Cd2265 Ce4186 Co2286 Cr2677 Cu3247
Units count count count count count count
Avge .00036 -.00015 .00057 -.00012 .00001 .00249
SOev .00001 .00018 .00017 .00008 .00007 .00005
iRSD 4.19756 117.472 31.2083 64.2845 683.498 2.34113
Eless Fe2714 K_7664 Li6707 Ng2790 Nn2576 «o2020
Units count count count count count count
Avge .00015 5.13044 .10713 .00019 .00004 .00003
SDev .00002 .09175 .00216 .00007 .00001 .00003
*RSD 15.5264 1.78837 2.01928 39.4158 30.4957 124.322
Eleis Na3302 N12316 PJ149 2203-1 2203-2 Sb2068
Units count count count count count count
Avge .00313 -.00156 -.00059 .00044 .00015 .00066
SDev .00568 .00032 .00022 .00113 .00032 .00021
«SD 181.451 20.5826 36.9268 253.261 210.464 32.4285
Eleiss 1960-1 1960-2 Snl899 Sr4215 Ti3349 T11908
Units count count count count count count
Avge -.00662 .00216 -.00052 .00031 .00033 -.00058
SOev .00156 .00027 .00005 .00001 .00022 .00009
*RSD 23.5681 12.56 11.3615 6.19176 65.6627 17.0359
Elens V_2924 Zn2062 S12881
Units count count count
Avge -.00032 .00003 .03211
SDev .00002 .00004 .00169
*RSD 8.1222 148.209 5.27207
96
-------
Anaivsis Reoort
Averaaes
Hon 07-28-97 06:51:53 AN oaae 2
Hethoa: TRIANG12 Saraole Na»e: ST03 Operator:
Run Tise: 07/28/97 01:29 Filename: 72797
Mode: IR Type: X Corr. Factor: 1.00000
Lab ID.: Cust. S»pl. ID.: Cust. ID.:
Elens Ag3280 A13082 AS1890 BJ496 Ba4934 Be3130
Units count count count count count count
Avge .45064 .02024 .05982 .18491 .30861 .31689
SDev .00082 .00002 .00014 .00261 .0009 .00204
*RSD .18382 .12777 .23797 1.41656 .29276 .64585
Elens Ca3179 Cd2265 Ce4186 Co2286 Cr2677 Cu3247
Units count count count count count count
Avge .02875 1.19708 .12656 .12483 .18327 .17785
SDev .00036 .01182 .00065 .00102 .00169 .00205
*RSD 1.26763 .988 .5162 .82189 .92358 1.15473
Elens Fe2714 KJ664 Li6707 Ng2790 Nn2576 Ho2020
Units count count count count count count
ftvge .0053 14.4762 8.50111 .0242 .1535 .09396
SDev .0001 .63224 .69665 .00026 .00134 .00035
*RSD 2.01091 4.36749 8.19492 1.08747 .87622 .37548
Eleis Na3302 Hi2316 P.2149 2203-1 2203-2 Sb2068
Units count count count count count count
Avge .10819 .43297 .02516 .2153 .10905 .1275
SDev .00533 .00181 .00013 .00474 .00196 .00058
*RSD 4.93029 .41886 .52872 2.20199 1.7984 .45507
Eleas 1960-1 1960-2 Snl899 Sr4215 Ti3349 T11908
Units count count count count count count
Avge .29341 .1736 .14097 .95076 1.27135 .03678
SDev .00291 .00262 .00105 .00113 .00464 .00025
*RSD .99267 1.51199 .75039 .11977 .36511 .70084
Elens VJ924 2n2062 Si2881 Pb2203 Sel960
Units count count count
Avge .04503 .12995 .06074
SDev .00018 .00203 .00255
XRSD .40876 1.5628 4.20073
97
-------
Mnaivsis Reoort
Averaaes
don 07-23-97 06:51:53 AM page 5
Nethod: TRIANGL2 Saiple Naine: STD3 Operator: DKH
Run Time: 07/28/97 01:34 Filenane: 72797
Noae: CONC TvDe: 0 Corr. Factor: 1.00000
Lao ID.: Cust. S«ol. ID.: Cust. ID.: 42298
Elans
Units
Avge
SDev
tRSD
[lens
Units
Avge
SDev
*RSD
Elens
Units
Avge
SDev
*RSD
Elets
Units
Avge
SDev
IRSD
Eleas
Units
Avge
SDev
*RSO
Eleis
Units
Avge
SDev
4RSD
Ag3280
ppb
996.2
4.129
.4145
Ca3179
ppb
990.0
11.07
1.119
Fe2714
ppb
980.6
22.94
2.34
Na3302
PP»
U10.51
.7479
7.119
1960-1
ppb
1011.
9.427
.9321
V.2924
ppb
995.1
2.342
.2353
A13082
ppb
988.8
6.355
.6427
Cd2265
ppb
993.9
5.352
.5385
K.7664
PP»
010.54
.7593
7.206
Ni2316
ppb
991.7
1.788
.1803
1960-2
ppb
998.4
24.24
2.428
Zn2062
ppb
991.1
12.63
1.274
AS1890
ppb
993.0
11.83
1.191
C84186
ppb
999.1
4.599
.4603
Li6707
ppb
Q1057.
91.7
8.678
P.2149
ppb
1000.
8.336
.8334
Snl899
ppb
993.9
2.048
.206
Si2881
ppb
Q9016.
917
10.17
8_2496
ppb
1008.
16.91
1.677
C02286
ppb
992.6
4.232
.4264
Mg2790
ppb
992.0
11.91
1.201
2203-1
ppb
997.9
21.58
2.163
Sr4215
ppb
989.2
7.46
.7542
Pb2203
ppb
998.9
11.43
1.144
8a4934
ppb
998.3
12.07
1.21
Cr2677
ppb
992.4
6.348
.6397
Hn2S76
ppb
992.0
2.92
.2943
2203-2
ppb
999.4
13.19
1.32
Ti3349
ppb
993.0
2.956
.2977
Sel960
ppb
1003.
16.72
1.6&8
Be3130
ppb
992.6
1.314
.1324
Cu3247
ppb
1000.
15.95
1.595
H02020
ppb
997.2
5.002
.5016
Sb2068
ppb
997.8
7.874
.7891
T11908
ppb
998.9
2.214
.2216
98
-------
Analysis teoort
Averaaes
Mon 07-28-^7 06:51:53 AM page 5
Methoa: TRIANGL2 Sauole Naue: ICV/CCV Ooerator: DKH
Run Time: 07/28/97 01:44 Filenane: 72797
floae: CONC Type: Q Corr. Factor: 1,00000
Lab 10.: Cust. Saol. ID.: Cust. 10.: 42298
Eleis
Units
Avge
SDev
*RSD
Elens
Units
Avge
SDev
VRSD
Eleis
Units
Avge
SOev
USD
Eleas
Units
Avge
SDev
tRSD
Eless
Units
Avge
SDev
*RSD
Elens
Units
Avge
SDev
*RS0
Ag3280
ppb
511.0
1.472
.2881
Ca3179
ppb
3562.1
9.446
1.681
Fe2714
ppb
498.0
19.45
3.905
Na3302
ppn
5.245
.2608
4.972
1960-1
ppb
505.1
4.359
.863
Ti3349
ppb
508.5
2.728
.5365
A13082
ppb
509.4
12.92
2.537
Cd2265
ppb
511.0
4.924
.9636
K_7664
ppm
5.146
.208
4.042
Ni2316
ppb
512.2
3.275
.6395
1960-2
ppb
516.8
3.283
.6352
T11908
ppb
514.4
3.061
.595
As 1890
ppb
509.3
2.697
.5291
Ce4186
ppb
512.2
2.603
.5083
Li6707
ppb
516.7
33.37
6.458
P.2149
ppb
514.1
4.682
.9108
Pb2203
ppb
508.6
7.532
1.481
V_2924
ppb
513.0
3.38
.6589
8.2496
ppb
510.9
4.634
.9069
Co2286
ppb
508.4
6.534
1.285
Mg2790
ppb
517.2
13.39
2.588
2203-1
ppb
503.8
13.03
2.587
Sel960
ppb
512.9
3.154
.615
Zn2062
ppb
519.6
9.463
1.821
834934
ppb
512.6
1.467
.2862
Cr2677
ppb
508.9
6.238
1.226
Hn2576
ppb
511.8
4.78
.9338
2203-2
ppb
511.0
4.787
.9368
Snl899
ppb
511.7
2.338
.457
Si2881
ppb
03939.
326.8
20.99
Be3130
ppb
506.1
3.051
.6029
Cu3247
ppb
516.8
3.085
.597
Mo2020
ppb
512.2
3.159
.6166
Sb2068
ppb
508.5
7.067
1.39
Sr4215
ppb
507.5
.8567
.1688
99
-------
Reoort
Averaaes
Mon 07-28-<>7 06:51:53 AM
oaae &
nethod: TRIANGL2 Sanple Name: IC8/CC8 Operator: DKH
Run Tine: 07/28/97 01:49 Filename: 72797
,loae: CONC Type: 0 Corr. Factor: 1.00000
L3D 10.: Cust. SsiDl. ID.: Cust. ID.: 42298
Eleis
Units
Avge
SOev
Elens
Units
Avge
SDev
tRSD
Elens
Units
Avge
SDev
WSD
Elens
Units
Avge
SDev
*RSD
Ag3280
ppb
-.9106
.9547
104.8
A13082
PP.
14.03
8.881
63.29
834934 y$e3130
ppb / ppb
.0706 .1299
.0£88 .1223
5.8 94.15
Ca3179 Cd2265
ppb ppb
.0615 .1794
.2994 .1463
486.6 81.55
8_2496
ppb
-1.390
3.459
248.7
ppb
.3087
2.012
651.7
Ce4186
ppb
-1.465
5.991
40
Cr2677 Cu3247
PPb ppb
.6206 .2338
.2885 .2139
46.49 91.48
Fe2714
ppb
3.273
15.1
461.4
U6707
ppb
.5136
.1771
34.49
Mg2790
ppb
5.675
4.068
71.68
Mn2576 H02020
ppb poo
.1037 .6568
.0979 .2353
94.47 35.83
Na3
'.2348 .8751
.3364 .502
143.3 57.37
2203-1
ppb
.9934
4.358
438.7
2203-2
ppb
1.766
2.832
160.4
Sb2068
ppb
2.281
3.777
165.6
1960-1
ppb
-.5685
5.787
1018
Pb2203
ppb
1.508
.7693
51
Snl899 Sr4215
ppb pob
.5419 .1013
91.43
EleuK^
Units
Avge
SDev
*RSD
Ti3349
*> — nnn —
upu
.1858
.0175
9.407
imoa^.
-^pc
06.613
4.173
63.1
-JT7924
ODD
-.3962
.5673
143.2
Zn2062
ppb
.2900
.3042
104.9
Si2881
pcb
Q-522.9
751.1
143.6
100
-------
Anaivsis Secor;
Averages
non 07-28-97 o»:51:53 AM cage 1
Metnoo: TRIANGL2 Sauole Name: ICB/CCB Ooerator: DKH
Run Tisne: 07/28/97 01:55 Filename: 72797
Hoae: CONC Tyoe: 0 Corr. Factor: 1.00000
LaD ID.: Cust. Siiol. ID.: Cust. ID.: 42298
Eless
Units
Avge
SDev
*RSD
Elems
Units
Avge
SDev
*RSD
Elems
Units
Avge
SOev
*RSD
Eleis
Units
Avge
SDev
*RSD
Eleins
Units
Avge
SDev
%RSD
tier;
Units
Avge
SDev
*RSD
Ag3280
ppb
.1290
1.597
1238
Ca3179
ppb
-.0182
1.471
8084
Fe2714
ppb
-7.863
25.37
329
Na3302
PP»
-.0317
.3326
1048
1960-1
ppb
1.799
4.794
266.4
TJ3349
ppb
.0098
.3345
3413
A13082
ODD
2.429
5.706
234.9
Cd2265
ppb
.0168
.0584
347.4
X.7664
PP«
.0537
.0105
19.56
Ni2316
ppb
.5994
.709
118,3
1960-2
ppb
-1.812
5.806
320.4
T11908
ppb
4.941
1.464
29.64
AS1890
ppb
-1.481
1.718
116
Ce4186
ppb
0-4.590
1.753
38.18
U6707
ppb
.1800
.1613
89.59
P.2149
ppb
2.532
5.703
225.2
Pb2203
ppb
.5315
1.691
318.2
V.2924
ppb
-.0592
.9745
1647
8_2496
ppb
-9.412
.8605
9.142
Co2286
ppb
.3581
.7797
217.8
Mg2790
ppb
2.317
6.085
262.6
2203-1
ppb
2.720
6.633
243.8
Sel960
ppb
-.6094
2.32
380.7
Zn2062
ppb
.0930
.1462
157.1
Ba4934
PDD
-.0251
.1266
504.4
Cr2677
ppb
-.1993
1.089
546.5
Mn2576
ppb
.0956
.1164
121.8
2203-2
ppb
-.5613
5.443
969.7
Snl899
ppb
.1067
.9978
935.3
S12881
ppb
fl-1504.
72.44
4.817
3e3130
ODD
.0937
.0804
85.77
Cu3247
ppb
-.3445
.8991
261
M02020
poo
.1769
1.021
576.9
Sb2068
opb
2.120
2.381
112.3
Sr4215
ppb
.0345
.057
165.1
101
-------
Analysis Reoort
Averaaes
lion 07-28-97 06:51:53 AM
oaoe a
Methoo: TRIANGi: Saoioie Name: ICSA8 Operator: OKH
Run Tine: 07/23/«7 02:00 Filenane: 72797
rtofle: CONC Type: Q Corr. Factor: 1.00000
UD ID.: Cust. Snol. ID.: Cust. ID.: 42298
Elens
Units
Avge
SDev
*RSO
EleiBS
Units
Avge
SDev
*RSD
Eleiis
Units
Avge
SDev
*RSD
Eleis
Units
Avge
SOev
tRSO
Eleas
Units
Avge
SDev
*RSD
Elens
Units
Avge
SDev
*RSD
Ag32SC
ppb
528.0
4.904
.9287
Ca3179
ppb
456200.
5156
1.13
Fe27U
ppb
171900.
407.7
.2371
Na3302
ODffl
06.180
.4896
7.922
1960-1
ppb
541.3
11.17
2.062
Ti3349
ppD
496.2
1.773
.3573
A13082
ppb
533600.
1666
.3122
Cd2265
ppb
461.3
1.127
.2442
K.7664
PP»
828.71
1.966
6.848
Ni2316
ppb
447.0
.207
.0463
1960-2
ppb
499.9
17.72
3.544
T11908
ppb
511.9
6.741
1.317
As 1890
ODD
509.2
3.397
.6671
Ce4186
ppb
493.1
5.71
1.158
Li6707
ppb
646.4
50.12
7.753
PJ149
ppb
504.4
5.776
1.145
Pb2203
pob
478.2
5.105
1.067
VJ924
PPb
494.7
1.515
.3064
8.2496
pob
514.3
8.52
1.657
Co2286
ppb
463.0
.1983
.0428
Mg2790
ppb
533900.
809.5
.1516
2203-1
ppb
514.1
6.919
1.346
Sel960
ppb
513.9
8.106
1.577
Zn2062
ppb
430.3
3.871
.8996
834934
ppb
513.1
6.393
1.246
Cr2677
ppb
476.8
1.614
.3384
Mn2576
ppb
455.6
.5328
.1169
2203-2
ppb
460.3
8,569
1.862
Snl899
ppb
493.4
3.627
.735
Si2881
ppb
08644.
762.8
8.826
Be3130
pob
482.7
.5072
.1051
Cu3247
PPb
525.6
10.96
2.085
M02020
ppb
492.9
2.028
.4113
Sb2068
ppb
498.7
10.17
2.04
Sr4215
pob
0495.7
4.147
.8366
102
-------
Anaivsis Reoort
Averaoes
rton 07-28-!'7 06:51:53 AM
page 9
Method: TRIANGL2 Sasple rtaae: 42298 MB Ocerator: DXH
Run Tine: 07/28/97 02:09 Filenaae: 72797
Mode: CONC Jyoe: S Corr. Factor: 1.00000
Lab 10.: Cust. Snol. ID.: Cust. ID.: 42298
Elets
Units
Avge
SDev
«SD
AS1890 8e3130
ppb ppb
L-3.490LO4W
l.W — T0393
54.94 26.35
Cd2265
Eleis N12316 Pb2203 Sb20^ Sel960
Units ppb ppb wro ppb
Avge L-.5858 L-.OSjX 4.550 L.9840
SOev 1.548 .373< 3.046 2.3
«SO 264.3
103
-------
Analysis Reoort Averages
Mon 07-28-97 06:51:53 AM page 10
Method: TRIAN6L2 Sample Name: 42298 LCS Qoerator: DKH
Run Tine: 07/28/97 02:13 Filenaie: 72797
Mode: CONC Type: S Corr. Factor: 1.00000
Lab ID.: Cust. Snipl. ID.: Cust. ID.: 42298
Elens
Units
Avge
SDev
*RSD
AS1890 8e3130 Cd2265 Co2286 Cr2677 Mn2576
ppb ppb ppb ppb ppb ppb
41.89 44.31 45.10 46.55 46.66 45.99
2.697 .2683 .5899 1.689 1.945 .5454
6.438 .6055 1.308 3.629 4.167 1.186
Elens
Units
Avge
SOev
*RSD
Ni2316 Pb2203
ppb ppb
45.33 52.49
.9438 1.074
2.082 2.046
Sb2068
ppb
52.65
4.992
9.48
Sel960
ppb
44.65
1.401
3.139
104
-------
»—•• cx
C-J B •-
CD O>
en -o *>
*- -o t*»
4^- o>^ CT- '—
-e»- • oo
ro -^o
cr- o
ro
«o
C-J
-o co
O>^ TD O-
o o- ro
<=>
>— o
o oo
cr> —* ^» t/>
C '-< ro CM
CO CO
B
O
-^j CT- ro
• ro
ro oo
C~> —rt I •
O ^—- OK c
-i i—• <=> J-
-I CD I **
;;» *— I
^ 30 ^
-n B - C
ro -o -<
ro -o 3K
en -o =3
-^~ Cyst o~ rO
O>* Ln en
Oo • —»j
4^. O^
CJl
-------
Analvsis Reoort
Averaaes
Mon 07-23-^7 06:51:53 AM page 12
Method: TRIAN6L2 Sasple Kane: 173-&0-1A.10 POS Ooerator: OKH
Run Tine: 07/28/97 02:23 Filenaie: 72797
node: CONC Type: 5 Corr. Factor: 1.00000
Lab ID.: Cust. Siol. ID.: Cust. ID.: 42298
eiens
Units
Avge
SDev
tRSD
AS1890
ppb
85.38
4.563
5.344
8e3130
ppb
46.21
.5478
1.186
Cd2265
ppb
759.2
10.88
1.433
Co2286
ppb
40.63
.3985
.9808
Cr2677
ppb
263.4
3.741
1.42
Mn2576
ppb
574.1
7.403
1.289
Eiens
Units
ftvge
SDev
tRSD
N12316
ppb
850.0
10.34
1.216
Pb2203
ppb
H143100.
3084
2.155
Sb2068
ppb
114.0
3.494
3.064
Sel960
ppb
210.2
3.711
1.765
106
-------
Anaivsis Reoort
Averages
rton 07-28-97 06:51:53 AM page 13
Ooerator: DXH
Methoa: TRIANGL2 Sanple Naie: 173-60-1A.10 L
Run Tiie: 07/28/97 02:27 Filenaie: 72797
Mode: CONC Type: S Core. Factor: 1.00000
Lab ID.: Oust. Supl. ID.: Cust. ID.: 42298
[less
Units
Avge
SDev
*RSD
Asl890
ppb
7.927
.7569
9.549
8e3130
opb
L.1356
.0502
37.01
Cd2265
ppb
153.1
2.745
1.792
Co2286
ppb
L-1.256
.658
52.39
Cr2677
ppb
48.99
1.509
3.08
Mn2576
ppb
108.4
2.068
1.908
Eleis
Units
Avge
SDev
*RSD
H12316
ppb
172.6
2.942
1.704
Pb2203
ppb
30780.
646.5
2.101
Sb2068
pob
14.47
2.317
16.02
Sel960
ppb
37.39
.3544
.948
107
-------
Analysis Recoct
Averages
Non 07-28-^7 06:51:53 AH oaae
Method: TRIANGL2 Samole Naine:
Run Tine: 07/28/97 02:32
Node: CONC Type: S Corr.
Lab ID.: Cust. Sipl. ID.:
173-60-2A ^ ^
Filena»eT7279^
Factor:
Cust.
Operator: DKH
1.00000
ID.: 42298
Elens
Units
Avge
SDev
«RSD
Asl890
ppb
43.27
2.737
6.325
8e3130
ppb
L.2496
.0181
7.233
Cd2265
ppb
674.6
2.263
.3354
Co2286
ppb
L.8551
.7339
85.83
Cr2677
ppb
171.7
.5759
.3354
Nn2576
ppb
561.1
2.043
.3642
Eleis
Units
Avge
SDev
\RSD
N12316
ppb
1166.
3.991
.3421
Pb2203
ppb
H134200.
1603
1.194
Sb2068
PPb
58.08
2.722
4.688
Sel960
ppb
186.6
1.213
.6498
108
-------
Analysis fteoort
Averages
Mon 07-28-°' 06:51:53 AM oaae 15
Methoa: TRIANGL2 Saddle Nane: 173-60-2A DA
Run Time: 07/28/97 02:37 Filenaue: 72797
Mode: CONC Type: S Corr. Factor:
Lab ID.: Cust. Siol. ID.: Cust.
Ooerator: DXH
1.00000
ID.: 42298
[lens
Units
Avge
SDev
tfiSD
Asl890
ppb
42.79
3.041
7.105
Be3130
ppb
L.2035
.013
6.392
Cd2265
ppb
670.0
4.388
.6549
C02286
ppb
1.169
.269
23.01
Cr2677
Kpb
170.7
.9995
.5855
Mn2576
ppb
559.3
2.887
.5162
Eleis N12316 Pb2203 Sb2068 Sel960
Units ppb ppb ppb ppb
Avge 1161. H133900. 63.09 187.6
SDsv 3.387 1219 2.267 3.807
tRSD .2917 .9106 3.593 2.03
109
-------
Analysis Reoort
Averaaes
Hon 07-28-97 06:51:53 AM page 16
ilethoa: TRIAN6L2 Saiole Nane: 173-60-3A
Run Tiie: 07/28/97 02:42 Filename: 72797
Mode: COHC Type: S Corr. Factor:
Lab ID.: Cust. Siol. ID.: Cust.
Operator: DKH
1.00000
ID.: 42298
Eleis
Units
Avge
SDev
IRSD
AS1890
ppb
38.96
3.603
9.25
8e3130
ppb
L.2132
.0341
16.01
Cd2265
PPb
726.3
4.549
.6259
C02286
ppb
L-7.951
.3931
4.944
Cr2677
ppb
174.5
.3425
.1963
Mn2576
ppb
1147.
4.577
.399
Eleis
Units
Avge
SDev
*RSO
Ni2316
PPb
664.2
1.525
.2297
Pb2203
ppb
H145200.
1733
1.194
Sb2068
ppb
63.04
3.865
6.131
Sel960
ppb
168.3
3.449
2.049
110
-------
Analysis Recoct
Averaaes
«on 07-28-97 06:51:53 Art page 17
Operator: DXH
rtetnod: TRIAN6L2 Saaole Naie: 173-60-4A
Run Tioie: 07/28/97 02:46 Filenaie: 72797'
Mode: CONC Type: S Corr. Factor: 1.00000
Lao ID.: Cust. Sip], ID.: Cust. ID.: 42298
Elans
Units
Avge
SDev
IRSD
As 1890
ppb
5.776
2.011
34.83
Be3130
ppb
L.0559
.035
62.55
Cd2265
ppb
L-5.083
.1337
2.63
C02286
ppb
L-13.71
.9953
7.258
Cr2677
ppb
115.5
1.695
1.468
Nn2576
ppb
140.3
1.579
1.125
tieis
Units
Avge
SDev
»SD
Ni2316
ppb
490.0
1.181
.241
Pb2203
ppb
270.5
72.89
26.94
Sb2068
ppb
62.16
3.565
5.735
Sel960
ppb
58.51
2.315
3.957
111
-------
Analysis Recoct Averages
lion 07-28-97 06:51:53 AM cage 18
Method: TRIANGL2 Sanole Nane: 173-60-5A Operator: DKH
Run Tiae: 07/28/97 02:51 Filenaie: 72797
Mode: CONC Type: S Corr. Factor: 1.00000
Lab ID.: Cust. Snol. ID.: Cust. ID.: 42298
El ens
Units
Avge
SDev
*RSD
AS1890
ppb
L3.659
1.007
27.51
8e3130
ppb
L-.0089
.02
224.2
Cd2265
ppb
L-7.418
.4816
6.492
Co2286
ppb
L-14.65
.609
4.156
Cr2677
ppb
105.6
.8667
.8208
Mn2576
ppb
55.73
.2182
.3915
Eleis
Units
Avge
SDev
*RSD
Ni2316
PPb
248.8
1.443
.5799
Pb2203
ppb
92.01
2.6
2.826
Sb2068
ppb
60.67
1.812
2.986
Sel960
ppb
52.01
2.545
4.894
112
-------
Anaivsis Recoct
Averaaes
rton 07-28-97 06:51:53 AM page 19
Metnod: TRIANGL2 Saacie Name: ICV/CCV Ooerator: DKH
Run Tiie: 07/28/97 02:5o Filenane: 72797
Moae: CONC Tyoe: Q Corr. Factor: 1.00000
Lab ID.: Oust. Sraol. ID.: Cust. ID.: 42298
Eleras
Units
Avge
SDev
tRSD
Ag3280
ppb
0333.4
289.1
86.72
A13082
ppb
0254.3
404.3
159
Asl890
PPD
0341.4
294.9
86.39
8.2496
ppb
398.4
343.7
86.28
834934
ppb
0338.7
292.9
86.5
8e3130
ppb
0329.1
285.4
86.72
Eleas
Units
Avge
SDev
Elens
Units
Avge
SDev
WSD
Eleas
Units
Avge
SOev
*RSD
Eleas
Units
Avge
SOev
*RSD
EleiBS
Units
Avge
SDev
*RSD
Ca3179
ppb
0362.6
308.5
85.07
Fe2714
ppb
Q304.1
285.6
93.91
U3247
286
ppb
Q329.7
285.5
86.58
C
ppb
Q333.0
288.1
86.51
L16707
PDD
0381.2
330.3
86.78
K.7664
ppl
03.814
3.1
81.28
Ni2316
ppb
0335.3
289.7
86.3
2203-1
ppb
318.2
274.5
86.26
03.560
3.108
87.31
Sel960
ppb
0330.2
285.8
86.56
1960-1
ppb
329.8
280.4
85.0
Pb2203
PPb
0332.5
286.1
86.04
T11908
ppb
0342.3
288.6
.17
Zn2062
ppb
0334.3
289.6
86.63
V.2924
ppb
0337.9
287.9
85.21
113
-------
Analysis -goort Averages
Mon 07-28-°7 Os:51:53 AM page 20
Method: TRIANGL2 Sanole Nate: ICV/CCV Goerator: DKH
Run Tiie: 07/28/97 03:01 Filenaie: 72797
Node: CONC Tyoe: 0 Corr. Factor: 1.00000
Lab ID.: Cust. Snol. ID.: Cust. ID.: 42298
Eleins
Units
Avge
SDev
*RSD
Elens
Units
Avge
SDev
*RSD
Eleus
Units
Avge
SDev
WSD
[lens
Units
Avge
SDev
*RSD
Elens
Units
Avge
SDev
*RSD
Eleis
Units
Avge
SDev
WSD
Ag3280
oob
512.8
1.48
.2886
Ca3179
ppb
0560.2
10.45
1.866
Fe2714
ppb
526.1
33.32
6.333
Na3302
ppi
5.222
.3299
6.318
1960-1
ppb
515.6
12.83
2.488
Ti3349
ppb
511.2
1.227
.2401
A13082
Dob
534.0
10.61
1.987
Cd2265
ppb
515.0
4.981
.9672
K.7664
PP»
5.167
.5142
9.951
N12316
ppb
517.6
4.002
.7732
1960-2
DDb
519.7
1.841
.3543
T11908
ppb
515.6
5.6
1.086
AS1890
ppb
514.8
8.001
1.554
C64186
ppb
520.9
1.755
.337
Li6707
ppb
520.2
71.41
13.73
PJ149
ppb
527.0
3.238
.6144
Pb2203
ppb
522.0
16.88
3.235
VJ924
ppb
516.4
1.428
.2765
8_2496
ppb
601.5
4.835
.8038
Co2286
ppb
509.4
4.831
.9483
Hg2790
ppb
526.8
14.79
2.807
2203-1
ppb
506.5
24.68
4.872
Sel960
ppb
518.3
4.814
.9287
Zn2062
ppb
519.3
11.8
2.273
Ba4934
ppb
514.9
7.528
1.462
Cr2677
ppb
514.2
6.418
1.248
Hn2576
ppb
512.3
3.15
.6149
2203-2
ppb
529.7
13.32
2.516
Snl899
ppb
501.7
1.396
.2783
SI2881
ppb
Q568300.
95250
16.76
8e3130
oob
505.5
2.051
.4056
CU3247
ppb
520.9
10.09
1.937
M02020
pob
513.3
2.984
.5813
Sb2068
ppb
516.2
3.935
.7623
Sr4215
ppb
507.2
5.095
1.005
114
-------
Analysis Reoort
Averaaes
Mon 07-28-97 06:51:53 AM cage 21
Method: TRIANGL2 Saaole Naae: IC8/CC8
Run Time: 07/28/97 03:07 Filenaie: 72797
Ooerator: OKH
Mode: CONC
Lab ID.
El ens
Units
Avge
SDev
IRSD
Elenis
Units
Avge
SDe'v
*RSD
Eleas
Units
Avge
SDev
*RSD
Eleis
Units
Avge
SDev
*RSD
Eleins
Units
Avge
SDev
*RSD
Eleis
Units
Avge
SDev
*RSD
Type: 0
Corr. Factor:
: Cust. S«Dl. ID.:
Ag3280
ppb
-.5381
2.423
450.2
Ca3179
ppb
-.5198
.4252
81.81
Fe2714
ppb
-1.532
5.476
357.4
Na3302
pps
-.1967
.7089
360.4
1960-1
ppb
1.693
4.044
238.8
Ti3349
ppb
.0763
.0849
111.3
A13082
ppo
10.77
7.647
71.01.
Cd2265
ppb
-.1183
.0856
72.42
K.7664
ppi
-.1537
.1549
100.8
Hi2316
ppb
.7096
.824
116.1
1960-2
ppb
1.284
3.393
264.2
T11908
ppb
Q6.402
1.551
24.23
Asl890
ppb
-2.631
1.125
42.77
C64136
ppb
-.3998
2.102
525.6
Li6707
ppb
-.3124
.3573
114.4
P.2149
ppb
2.838
2.979
104.9
Pb2203
ppb
.1877
1.378
733.8
V.2924
ppb
.5162
.8914
172.7
8.2496
ppD
49.35
10.24
20.75
C02286
ppb
.7076
.408
57.66
Mg2790
ppb
4.448
3.893
87.53
2203-1
ppb
-.2262
9.288
4106
Sel960
ppb
1.420
1.528
107.5
Zn2062
ppb
-.0788
.2477
314.5
Cust.
8a4934
ppb
.0412
.0826
200.5
Cr2677
ppb
.8896
.5825
65.48
Mn2576
ppb
.0141
.0681
482.4
2203-2
ppb
.3944
6.581
1669
Snl899
ppb
-.0099
1.046
10580
Si2881
ppb
0241100.
24940
10.34
1.00000
ID.: 42298
8e3130
opb
.1042
.0123
11.85
CU3247
pob
-.5535
.4732
85.49
«o2020
ppb
-.2172
.532
244.9
Sb2068
ppb
.9105
.528
57.98
Sr4215
ppb
-.0079
.0335
423.2
115
-------
Analvsis Recort
Averaaes
Hon 07-28-<>7 06:51:53 AM page 22
Method: TRIANGL2 Samole Name: 173-60-6A Operator: DKH
Run Ti«e: 07/28/97 03:13 Filenaie: 72797
Node: CONC Type: S Corr. Factor: 1.00000
Lab ID.: Cust. Sipl. 10.: Cust. ID.: 42298
Elens
Units
Avge
SDev
*RSD
AS1890
ppb
L-1.483
3.423
230.8
8e3130
ppb
L.0058
.0279
481.1
Cd2265
ppb
L-.5303
.107
20.18
Co2286
ppb
L-1.436
.2428
16.9
Cr2677
ppb .
12.07
.3395
2.812
Nn2576
ppb
15.69
.0202
.1289
Elens N12316 Pb2203 Sb2068 Sel960
Units ppb ppb ppb ppb
Avge 6.064 5.342 13.834 3.383
SDev .6646 .1131 2.453 1.11
*RSD 10.96 2.118 63.98 32.82
116
-------
Anaivsis Reoort
Averaaes
(ion 07-28-97 06:51:53 AM oaae 23
flethod: TRIANGL2 Sanole Naie: 173-60-11A
Run Tine: 07/28/97 03:17 Filenaie: 72797
Node: CONC Type: S Corr. Fac:or:
Lab 10.: Cust. Suol. 10.: Cust.
Operator: OKH
1.00000
ID.: 42298
Eleis
Units
Avge
SDev
*RSD
AS1890
ppb
5.039
2.56
50.8
8e3130
ppb
1.1523
.0362
23.78
Cd2265
ppb
L-9.533
.4478
4.698
C02286
ppb
L-18.19
1.609
8.85
Cr2677
ppb
112.0
1.679
1.499
Hn2576
ppb
38.53
.4482
1.163
fleas
Units
Avge
SOev
*RSD
N12316
ppb
234.0
3.214
1.373
Pfa2203
ppb
18.77
.6581
3.506
S52068
ppb
66.55
5.838
8.773
Sel960
ppb
60.49
2.417
3.995
117
-------
ftnalvsis Recort
Averaaes
Mon 07-28-97 06::i:53 AH page 24
Method: TRIANG12 Saaole Naae: 173-60-12A
Run Tiie: 07/28/97 03:22 Filenaie: 72797
Hode: CONC Type: S Corr. Factor:
Lab ID.: Cust. Siol. ID.: Cust.
Operator: DKH
1.00000
ID.: *2298
tless
Units
Avge
SDev
tRSD
Asi890 8e3130 Cd2265 Co2286 Cr2677 Nn2576
ppb ppb ppb opb ppb ppo
141.5 L-1.343 861.0 L-.5110 841.9 13330
2.25 .1158 9.226 2.907 8.592 122.1
1.589 8.619 1.072 568.9 1.021 .9153
Eleis
Units
Avge
SDev
IRSD
NJ2316
PPb
1193.
10.11
.8473
Pb2203
PPb
H158900.
1978
1.245
352068
ppb
124.7
5.863
4.7
Sel960
ppb
347.3
1.792
.5161
118
-------
Anaivsis Recoct
Averaaes
Mon 07-28-97 06:Si::3 AH paae 25
Operator: DKH
Method: TRIANGL2 Saiiole Naae: 173-60-13A
Run Tine: 07/28/97 03:27 Filenaie: 72797
Mode: CONC Type: S Corr. Factor: 1.00000
Lab ID.: Cust. S»ol. ID.: Cust. ID.: 42298
Elens
Units
Avge
SDev
tRSD
AS1890
ppb
184.3
4.589
2.489
8e3130
ppb
L-2.734
.0387
1.414
Cd2265
ppb
308.3
8.328
1.092
C02286
ppb
13.84
.927
6.696
Cr2677
ppp
1009.
10.18
1.009
Hn2576
ppb
18020
192
1.065
El ems
Units
Avge
SDev
*RSD
N12316
ppb
828.5
7.001
.845
Pb2203 S52068
ppb ppb
H156900. 99.30
2725 4.828
1.737 4.862
Sel960
ppb
405.6
9.721
2.396
119
-------
Analysis Reoort
Averaaes
Mon 07-28-97 06:51:53 AM oaae Zc
Method: TRIANGL2 Samole Nane: 173-60-14A Ooerator: OKH
Run Tiie: 07/28/97 03:31 Filenaie: 72797
Mode: CONC Type: S Corr. Factor: 1.00000
Lab 10.: Cust. Sipl. ID.: Cust. ID.: 42298
Eleis
Units
Avge
SDev
*RSD
Asl890
ppb
201.0
2.766
1.376
Be3130
ppb
L-2.385
.1341
5.621
Cd2265
ppb
848.1
7.088
.8358
C02286
ppb
18.66
1.539
8.249
Cr2677
ppb
998.0
7.89
.7906
Mn2576
ppb
19000
153.3
.8069
Eleis N12316 Pb2203 Sb2068 Sel960
Units ppb ppb ppb ppb
Avge 869.8 H165700. 90.56 322.3
SOev 4.444 806 4.285 8.043
*RSD .511 .4863 4.731 2.496
120
-------
Anaivsis Reoort
Averages
Hon 07-28-97 06:51:53 AM cage 27
hethod: TRIANGL2 Sanole Nane:
Run Time: 07/28/97 03:36
Mode: CONC . Type: S
Lab ID.: Cust. S»pl. ID.:
173-60-18
Fij
Eleis Asl890 8e3130
Units ppb ppb
Avge L-.4306 L.0977
SDev 2.127 .0685
*RSD 494 70.12
Eleis N12316 Pb2203 yfl>2068
Units ppb ppb /ppb
Avge 38.80 12*8 4.806
SDev .2062 9O6 4.14
WSO .5314 /73.9S 86.14
Sel960
ppb
171.3
2.139
1.248
Operator: DKH
'0000
42298
121
-------
Analysis Reoort
Averaaes
Mon 07-28-97 06:51:53 Ah oaae 28
Netnod: TRIANGL2 Saiole Naae: 173-60-18 POS Operator: OKH
Run Ii«e: 07/28/97 03:41 Filenane: 72797
Hooe: CONC Type: S Corr. Factor: 1.00000
Lao ID.: Cust. Saol. 10.: Cust. ID.: 42298
Eleis
Units
ftvge
SDev
*RSO
AS1890
ppb
' 44.31
2.669
6.023
6e3130
ppb
46.56
.3235
.6948
Cd2265
ppb
53.00
.5918
1.117
Co2286
ppb
47.22
.9871
2.09
Cr2677
ppb
75.38
1.614
2.141
Hn2576
ppb
148.5
3:817
2.57
Eleis
Units
Avge
SDev
IRSD
Ni2316
ppb
86.68
1.368
1.578
Pb2203
ppb
115.9
1.938
1.672
Sb2068
ppb
49.78
1.837
3.689
Sel960
ppb
210.8
1.572
.7459
122
-------
Analysis Recoct
Averaaes
don 07-28-97 06:51:53 AM page 29
Method: TRIANGL2 Saaole Mane: 173-60-18 L Ooerator: OKH
Run Time: 07/28/97 03:46 filenaie: 72797
Mode: CONC Tyce: S Corr. Factor: 1.00000
Lab ID.: Cust. Sipl. ID.: Cust. ID.: 42298
Ele«s
Units
Avge
SDev
«SD
Asl890 B83130 Cd2265 Co2286 Cr2677 Hn2576
ppb ppb ppb ppb ppb ppb
1-1.318 L.0692 1.119 L.1816 5.556 19.98
.5984 .0714 .0553 1.069 1.28 .0988
45.42 103.2 4.943 588.5 23.04 .4945
Eleis
Units
Avge
SDe'v
*RSD
Ni2316
ppb
7.849
.6526
8.315
Pb2203
ppb
18.60
3.687
19.82
Sb2068
ppb
L.5217
3.156
604.9
Sel960
ppb
36.70
2.291
6.242
123
-------
Anaivsis Reoort Averaaes
Won 07-28-97 06:51:53 AH page 30
Method: TRIAN6L2 Saiole Name: 173-60-28 Ooerator: DXH
Run Ti«e: 07/28/97 03:50 Filenaw: 72797
Mode: CONC Type: S Corr. Factor: 1.00000
Lab ID.: Cust. Sipl. 10.: Cust. ID.: 42298
Eleis
Units
Avge
SDev
*RSD
As 1890
ppb
L-2.804
1.163
41.48
8e3130
ppb
L.0652
.1032
158.3
Cd2265
ppb
L-.3177
.3963
124.7
C02286
ppb
L-1.593
.7373
46.29
Cr2677
ppb
12.89
.8695
6.746
«n2576
ppb
205.6
1.125
.5472
Eleis
Units
ftvge
SDev
*RSD
Ni2316
ppb
4.377
.9922
22.67
PD2203
ppb
9.816
2.196
22.38
SD2068
ppb
L2.228
3.903
175.2
serno
ppb
139.6
2.119
1.518
124
-------
Analysis Reoort
Averaaes
rton 07-28-97 06:51:53 AH oaae 31
Method: TRIANGL2 Sanole Name: 173-60-28 DA Operator: DKH
Run line: 07/28/97 03:55 Filenaie: 72797
Mode: CONC Type: S Core. Factor: 1.00000
Lab 10.: Cust. Sspl. ID.: Cust. ID.: 42298
Elans
Units
Avge
SDev
*RSD
Asl890
pob
L-4.576
1.616
35.32
Be3130
ppb
L.0806
.0559
69.4
Cd2265
ppb
L-.3430
.2883
84.05
C02286
ppfa
L-1.807
.8453
46.79
Cr2677
ppb
12.37
.2993
2.421
Mn2576
ppb
206.7
.4862
.2352
Eleis N12316 Pb2203 Sb2068 Sel960
Units ppb ppb ppb ppb
Avge 4.301 9.255 LI.696 134.4
SDev .4849 .7742 1.648 1.42
*RSD 11.27 8.364 97.15 1.056
125
-------
Anaivsis Reoort
Hveraaes
flon 07-28-97 06:51:53 AM oaae 32
fletnoa: TRIAN6L2 Saaole Nane: 1CV/CCV Ocerator: OKH
Run Tine: 07/28/97 04:00 Filenaie: 72797
Moce: CONC Tyoe: 0 Corr. Factor: 1.00000
Lab ID.: Cust. Stool. ID.: Cust. ID.: 42298
Elens
Units
Avge
SDev
*RSD
Eleas
Units
Avge
SDev
tRSD
Elens
Units
Avge
SDev
*RSD
Eleis
Units
Avge
SDev
*RSD
ties;
Units
Avge
SDev
iRSD
Ele»s
Units
Avge
SDev
*RSD
Ag3280
pob
511.3
1.24
.2425
Ca3179
ppb
544.5
7.765
1.426
Fe2714
ppb
504.8
23.77
4.709
Na3302
pps
5.415
.2764
5.104
1960-1
ppb
496.9
2.499
.503
Ti3349
ODD
503.7
1.539
.3055
A13082
ODD
510.9
12.34
2.416
Cd2265
ppb
510.0
3.215
.6305
K.7664
ppa
05.514
.2082
3.776
Ni2316
ppb
513.4
2.484
.4839
1960-2
pob
506.7
5.267
1.039
T11908
ODD
511.0
1.18
.2309
AS1890
ppb
510.1
6.632
1.3
Ce4186
ppb
513.0
4.246
.8276
Li6707
ppb
Q559.7
34.58
6.178
PJ149
ppb
518.3
7.817
1.508
Pb2203
ppb
508.9
5.361
1.053
V.2924
ppb
510.3
1.974
.3868
BJ496
pob
537.5
5.434
1.011
C02286
ppb
502.3
4.075
.8113
Mg2790
ppb
518.9
14.94
2.878
2203-1
ppb
484.8
5.862
1.209
S61960
ppb
503.5
4.304
.855
Zn2062
ppb
506.3
7.505
1.482
834934
pob
511.6
5.664
1.107
Cr2677
ppb
505.9
5.99
1.184
Hn2576
ppb
501.0
2.929
.5847
2203-2
ppb
521.0
5.172
.9926
Snl899
ppb
497.7
3.801
.7638
S12881
ppb
041400.
10370
25.05
8e3150
pob
501.5
1.902
.3793
Cu3247
ppb
518.6
6.79
1.309
M02020
ppb
513.0
1.993
.3886
Sb2068
ppb
508.5
4.934
.9702
Sr4215
ppb
501.0
3.402
.6791
-------
Anaivsis Reoort
Averaaes
rton :'-28-<»7 06:51:53 AM oaae 33
flethod: TRIAN6L2 Saisole Nanie: IC8/CC8 Operator: OKH
Run Time: 07/28/97 04:05 Filenaie: ll'^l
Mode: CONC Type: Q Corr. Factor: 1.00000
Lab ID.: Cust. Sniol. ID,: Cust. ID.: 42298
Elens
Units
Avge
SDev
*RSD
AQ3280 A13082 fls!890 8.2496 8a4934 Be3130
ODD opt) pob ppb ODD ppb
-.7678 15.12 -.7294 Ijjj — -r«73~"~"7l837
.4105 4.446 2.101 4.697 .201 .0122
53.46 29.39 288.1 35.23 1628 6.646
Eleis
Units
Avge
SDev
*RSD
Ca3179
ppb
-2.090
2.02
96.66
Cd2265
ppb
-.0871
.2122
243.6
C64186
ppb
fl-3.097
8.23
265.7
C02286
ppb
-.1727
1.139
659. 4 /
Cr2677
poo
-.ooX
LM6
"51370
CuJXV
/P&>
-1.017
1.178
115.9
Eleits
Units
Avge
SDev
*RSD
Fe2714
ppb
-8.664
23.33
269.3
X.7664
ppn
-.2953
.1751
59.3 /
Li6707
ppb /
-X301
/?,%!
62.95
X2"o
ppb
2.387
13.58
568.7
Bn2576
ODD
.0193
.1395
723.6
M02020
ppb
-.2152
.2407
111.8
Elens
Units
Avge
SOev
«SD
Na3302 )tt2316 P_2149 2203-1 2203-2 Sb2068
ppi /ppb ppb ppb ppb ppb
-.26/3 .6011 3.558 1.173 1.890 1.221
.1402 .7171 11.46 6.212 3.432 3.585
6/12 119.3 322.2 529.7 181.6 293.6
Eleis
Units
Avge
SDev
*RSD
/1960-1
ppb
7.616
367.5
1960-2
ppb
_2_£
4.644
178.5
Elens
Units
Avge
SOev
*RSD
Ti3349
pob
.0418
.4309
1030
T11908
pob
06.439
3.381
52.51
V.2924
ppb
.4591
1.383
301.2
Zn2062
ppb
.0903
.7609
843.1
Si2881
pcb
Q18040.
2560
14.19
Sel960 JjUBS*—-ST??l5
pob ppb
2.425 .3678 -.0208
.8376 1.436 .1058
34.54 390.4 507.8
127
-------
Analysis Report Averaaes
rton 07-28-97 06:51:53 Afl page 34
Method: TRIANGL2 Saaole Name: ICB/CCS Operator: DKH
Run Time: 07/28/97 04:16 Filenane: 72797
Mode: CONC Type: 0 Corr. Factor: 1.00000
Lao ID.: Cast. Snipl. ID.: Cust. ID.: 42298
Elenis
Units
Avge
SDev
*RSO
Ag3230 A15082 Asl890 8.2496 8a4934 Be3130
ppb ppo ppb ppb ppb ppb
Q2.514 15.22 4,675 7.568 .2357 .1255
7.674 53.95 7.68 5.746 -4705 L.U7<^
305.3 354.5 164.3 75.92^-WTT 293. 2"
Elens
Units
Avge
SDev
tRSD
Ca3179
ppb
3.116
4.429
142.2
Cd2265
ppb
.4111
.6871
167.1
CI7I86
ppb
07.880
16.59
210.6
Co2286
ppb
01.842
1.974
107.2 >
Cr2677
ppb .
1.9MT
1/591
/82.21
Cy3247
/PPb
-.0054
3.73
68690
Elems
Units
Avge
SDev
tRSD
Fe2714
ppb
29.82
46.3
155.3
K.7664
DDia
.0714
.1553
217.6
Li6707
PPb >
.0927
.2*«
/62.8
K?2790
/ppb
19.09
23.88
125.1
Mn2576
ppb
.3555
.291
81.84
«o2020
ppb
1.320
1.306
98.92
Elens
Units
Avge
SDev
*RSD
19/0-1 1960-2
P/b ppb
[-34.93 23.05
4^,89
134^ 112.2
Pb2203
2.065
68
03.742
1.662
44.41
Eleiiis
Units
Avge
SDev
«SD
Ti3349
ppb
.5091
.9514
186.9
T11908
ppo
Q6.528
7.509
115
V_2924
ppb
02.950
2.639
89.46
Zn2062
ppb
1.420
1.187
83.62
Si2881
ppb
015030.
3848
25.61
Eleis
Units
Avge
SDev
*RSD
Na3302 Ni23f6 P.2149 2203-1 2203-2 Sb2068
ppra pot ppb ppb ppb ppb
.9772 /6236 4.904 -12.43 10.76 Q12.64
2.661/3.091 20.69 9.825 7.888 7.456
212. V 495.7 421.9 79.03 73.31 SS**T
128
-------
Analysis Reoort
Averages
Mon 07-28-^7 06:51:53 AM oaae 35
Method: TRIANGL2 Saraole Name: ICB/CC8 Operator: DKH
Run Tine: 07/28/97 04:21 Filenase: 72797
Mode: CONC Type: Q Corr. Factor: 1.00000
Lab ID.: Cust. S»ol. ID.: Cust. ID.: 42298
Hens
Units
Avge
SOev
«SD
Elfins
Units
Avge
SDev
*RSD
El ens
Units
ftvge
SDev
%RSD
Elens
Units
Avge
SDev
*RSD
Elens
Units
ftvge
SDev
*RSD
Elens
Units
Avge
SOev
*RSD
Ag3280
ppb
-.9562
1.836
192
Ca3179
ppb
-1.256
1.926
153.3
Fe2714
ppb
3.778
21.98
581.8
Na3302
ppB
-.4738
.6131
129.4
1960-1
ppb
-4.676
2.747
58.74
TJ3349
ppb
.2819
.3939
139.7
A13082
ppb
28.54
14.01
49.08
W2265
ppb
.1380
.1123
81.39
KJ664
PP»
-.2321
,2549
109.8
Ni2316
ppb
.4907
.6086
124
1960-2
ppb
4.869
3.239
66.51
T11908
ppb
4.070
3.814
93.71
Asl890
ppb
-1.108
1.828
164.9
C64186
ppb
-1.734
2.992
172.6
Li6707
ppb
-.5083
.5629
110.7
P_2149
ppb
1.692
5.029
297.3
Pb2203
ppb
.3991
.8234
206.3
V.2924
ppb
.7638
.965
126.3
8.2496
ppb
4.208
4.281
101.7
Co2286
pob
.8572
.9639
112.4
«g2790
ppb
7.832
11.65
148.7
2203-1
ppb
-3.709
8.647
233.1
Sel960
ppb
1.691
1.717
101.6
Zn2062
ppb
.3474
.2959
85.18
6a4934
ppb
.1543
.2196
142.3
Cr2677
ppb
.8790
1.549
176.2
Mn2576
ppb
.1291
.1503
116.4
2203-2
ppb
2.450
5.53
225.7
Snl899
ppb
-.4069
1.965
482.9
Si2881
ppb
014970.
3553
23.73
8e3130
ppb
.2442
.0568
23.27
CU3247
ppb
.2667
1.711
641.8
Ho2020
ppb
.4505
1.252
277.8
Sb2068
ppb
2.988
2.816
94.23
Sr4215
ppb
.0632
.0945
149.5
129
-------
Analysis Report Averages
Mon 07-28-97 06:51:53 Ah page 36
Method: TRIAN6L2 Saaole Na»e: 173-60-38 Ooerator: DKH
Run Tiie: 07/28/97 04:27 Filenane: 72797
Mode: CONC Type: S Corr. Factor: 1.00000
Lab ID.: Cust. S»pl. ID.: Cust. ID.: 42298
Elens
Units
Avge
SDev
*RSD
AS1890
ppb
L-3.089
3.463
112.1
Be3130
ppb
L.2012
.0903
44.85
Cd2265
ODD
L-.0304
.1314
431.6
C02286
ppb
L-.9347
.811
86.77
Cr2677
PDD
16.98
1.174
6.912
Mn2576
ppb
2682.
40.94
1.526
Elens
Units
Avge
SDev
*RSO
N12316
ppb
4.349
.7839
18.02
Pb2203
PPb
16.68
.4601
2.759
Sb2068
ppb
4.028
3.634
90.24
Sel960
PPb
161.2
3.532
2.191
130
-------
Analysis Reoort
fiveraaes
ion 07-28-37 06:51:53 AH oaae 37
Method: TRIANGL2 Sanple Name: 173-60-48.4A Ooerator: OKH
Run Tine: 07/28/97 04:32 Filenaee: 72797
Node: CONC Tyoe: S Corr. Factor: 1.00000
Lab ID.: Cust. Supl. ID.: Cust. 10.: 42298
Eleis
Units
Avge
SDev
*RSD
Asl890
ppb
L-3.540
2.223
62.8
Be3130
ppb
L.0500
.0117
23.48
Cd2265
ppb
L.2610
.0647
24.79'
Co2286
ppb
L-.9045
.1876
20.74
Cr2677
ppb
12.97
.1127
.8688
Nn2576
ppb
157.4
.2775
.1763
Eleis N12316 Pb2203 Sb2068 Sel960
Units ppb ppb ppb ppb
Avge 4.587 39.87 1-1.279 12.05
SDev .4635 .5212 1.966 .2594
*RSD 10.11 1.307 153.7 2.153
131
-------
Analvsis Reoort
Averaaes
Mon 07-28-97 06:51:53 AM oaae 38
Method: TRIAN6L2 SaiDle Name: 173-60-58.5A Ooerator: DKH
Run Tine: 07/28/97 04:36 Filenane: 72797
Mode: CONC Type: S Corr. Factor: 1.00000
Lab ID.: Cust. Siol. ID.: Cust. 10.: 42298
Elens
Units
Avge
SOev
*RSO
AS1890 Be3130 Cd2265 Co2286 Cr2677 Mn2576
ppb ppb ppb ppb ppb ppb
L-4.576 L.1294 L.3735 L-1.180 12.65 1241.
1.686 .0363 .2092 .4749 .307 1.498
36.85 28.09 56.02 40.26 2.428 .1207
Elens
Units
Avge
SOev
*RSD
N12316
ppb
3.475
.6575
18.92
Pb2203
ppb
129.9
1.092
.8406
Sb2068
PPb
L-.5355
2.413
450.5
Sel960
ppb
10.09
1.963
19.46
132
-------
Analysis Seoort
Averaaes
lion 07-28-97 06:51:53 AM oaae 59
Method: TRIANGL2 Sanole Nane: 173-60-6A,6C Ooerator: DKH
Run Ti»e: 07/28/97 04:41 Filenaie: 72797
Mode: CONC Type: S Corr. Factor: 1.00000
Lab ID.: Cust. S»ol. ID.: Cust. ID.: 42298
[lens
Units
Avge
SDev
%RSD
Asl890 Be3130 Cd2265 Co2286 Cr2677 Mn2576
ppb ppb ppb ppb ppb ppb
L-3.656 L.1687 L-.2888 L-.5942 8.229 11.14
.6 .0229 .1213 .6661 .4422 .7328
16.41 13.54 42.01 112.1 5.373 6.579
Eless
Units
Avge
SDev
*RSO
Ni2316
ppb
L2.188
1.049
47.93
P62203
ppb
4.697
1.429
30.42
Sb2068
ppb
L2.279
1.8
79.01
Sel960
ppb
L2.176
1.36
62.5
133
-------
Analysis Recoct
Averaaes
Mon 07-28-97 06:51:53 AM oaae 40
flethod: TRIANGL2 Sasole Mane: 173-60-7 Operator: DKH
Run Tine: 07/28/97 04:46 Filename: 72797
Mode: CONC Type: S Corr. Factor: 1.00000
Lao 10.: Cust. Siol. ID.: Cust. ID.: 42298
El ems
Units
Avge
SOev
*RSD
AS1890
ppb
L-6.245
1.05
16.81
8e3130
ppb
L.1081
.0482
44.57
Cd2265
ppb
L-.3040
.2221
73.07
C02286
ppb
L-.9122
.9438
103.5
Cr2677
pob
9.524
1.321
13.87
Mn2576
pob
35.88
.0577
.1607
Eleas
Units
Avge
SDev
*RSD
Ni2316
ppb
4.083
1.002
24.54
Pb2203
ppb
6.893
.3305
4.795
SD2068
ppb
L-1.340
3.138
234.2
Sel960
ppb
L-1.281
1.149
89.72
134
-------
Analysis Reoort Averages
Mon 07-28-97 06:51:53 AM page 41
Method: TRIANGL2 Saiole Nane: 173-60-11A,11B Operator: DKH
Run Time: 07/28/97 04:51 Filenaie: 72797
Mode: CONC Type: S Corr. Factor: 1.00000
Lab ID.: Cust. S«ol. 10.: Cust. ID.: 42298
Ele»s
Units
Avge
SDev
WSO
Asl890
opb
L-3.108
.9647
31.03
883130
ppb
L.0965
.021
21.71
Cd2265
ppb
L-.1653
.0846
51.2
Co2286
ppb
L-.9931
.1717
17.29
Cr2677
ppb
5.012
.316
6.304
Mn2576
ppb
29.92
.0632
.2113
Units
Avoe
SOev
*RSD
N12316 Pb2203 Sb2068 Sel960
ppb ppb ppb ppb
LI. 815 8.588 7.076 L-.6281
.4165 .8216 .8807 1.755
22.95 9.567 12.45 279.3
135
-------
Analysis Recort
Averaaes
Hon 07-28-97 06:51:53 AM cage 42
Netnod: TRIANGL2 Saaole Na«e: 173-60-128 Ooerator: OKH
Run Tine: 07/28/97 04:55 Filenaie: 72797
Hoce: CONC Type: S Corr. Factor: 1.00000
Lao ID.: Cust. S»pl. ID.: Cust. ID.: 42298
Ele*s
Units
Avge
SDev
tRSD
AS1890
ppb
L-1.114
1.431
128.4
8e3130
ppb
L.0168
.0118
70.28
Cd2265
ppb
7.374
.2877
3.902
Co2286
ppb
L.5574
.2973
53.33
Cr2677
ppb
58.85
.3246
.5515
Mn2576
ppb
437.6
1.289
.2945
Eleis
Units
Avge
SDev
tRSD
N12316
ppb
40.03
.9589
2.396
Pb2203
ppb
808.6
11.26
1.393
Sb2068
ppb
L.1127
.7468
662.3
Sel960
ppb
126.5
.7997
.6321
136
-------
Analvsis Recoct
Averaaes
Mon 07-28-^ 06:51:53 AM oaae 43
Method: TRIANGL2 Sauole Naae: 173-60-138 Operator: DXH
Run Tine: 07/28/97 05:00 Filena«e: 72797
Mode: CONC Type: S Corr. Factor: 1.00000
Lab ID.: Cust. Saoi. ID.: Cust. ID.: 42298
Elens
Units
Avge
SOev
IRSD
Asl890 8e3130 Cd2265 Co2286 Cr2677 Mn2576
ppb ppb ppb ppb ppb ppb
L-2.825 L.0549 L-.3269 L-1.497 12.70 52.15
3.876 .1471 .2472 1.391 2.472 .596
137.2 268.1 75.63 92.9 19.47 1.143
Elens
Units
Avge
SOev
*RSD
N12316
ppb
8.878
1.328
14.96
Pb2203
ppb
10.71
1.283
11.98
Sb2068 Sel960
ppb ppb
L-2.560 161.4
6.306 .5137
246.3 .3183
137
-------
Analvsis Reoort
Averages
Mon 07-28-97 06:51:53 AH page 44
Method: TRIANGL2 Saaple Nane: 173-60-148 Operator: OKH
Run Tiie: 07/28/97 05:05 Filenaie: 72797
Mode: CONC Type: S Corr. Factor: 1.00000
Lab ID.: Cust. S«ol. ID.: Cust. ID.: 42298
Eless
Units
Avge
SDev
*RSD
Asl890
ppb
L-4.527
3.684
81.37
8e3130
ppb
L.0736
.0566
76.93
Cd2265
ppb
L-.4105
.1664
40.53
C02286
ppb
L-1.021
.5497
53.86
Cr2677
ppb
15.39
.6958
4.52
Mn2576
pob
97.23
.6805
.6999
Eless
Units
Avge
SDev
*RSD
Hi2316
ppb
3.670
.4769
13
Pb2203
ppb
10.37
1.7
16.39
Sb2068
ppb
L-1.563
1.971
126.1
Sel960
ppb
158.4
7.704
4.864
138
-------
Analysis Reoort
Averaaes
rton 07-23-97 06:51:53 AM page 45
Method: TRIANGL2 Saiole Name: 42298 H8 Operator: DKH
Run Tine: 07/28/97 05:19 Filenaie: 727
-------
Analysis Recoct
Averaaes
(ion 07-23-^7 06:51:53 AH oaae 46
rtethoa: TR1AN6L2 Sanole Nane: ICV/CCV Ooerator: OKH
Run Tine: 07/28/97 05:25 Filenaiae: 72797
Mode: CONC Type: 0 Corr. Factor: 1.00000
Lab ID.: Cust. Sid. 10.: Cust. ID.: 42298
Elems
Units
Avge
SDev
tRSD
Elens
Units
Avge
SDev
*RSD
Elems
Units
Avge
SDev
*RSD
Eleis
Units
fivge
SDev
*RSD
Eleis
Units
Avge
SDev
*RSD
Elenis
Units
Avge
SDev
*RSO
Ag3280
ppb
513.0
1.092
.2129
Ca3179
ppb
Q551.0
13.13
2.384
Fe2714
ppb
493.6
32.3
6.544
Ha3302
ppffl
5.002
.7986
15.97
1960-1
ppb
497.1
3.648
.7339
Ti3349
ppb
506.2
1.112
.2197
A13082
ppb
528.6
7.614
1.44
Cd2265
ppb
510.9
7.129
1.396
K_7664
ppi
5.191
.5372
10.35
Ni2316
PPb
512.9
5.997
1.169
1960-2
ppb
504.6
13.04
2.584
T11908
ppb
506.3
6.378
1.26
Asl890
PPb
507.7
4.162
.8197
Ce4l86
ppb
511.8
4.211
.8227
Ii6707
ppb
518.8
75.58
14.57
P.2149
PPb
518.7
16.05
3.094
Pb2203
ppb
505.5
9.766
1.932
V.2924
ppb
509.7
2.611
.5123
8.2496
PPb
504.8
9.5
1.882
Co2286
ppb
501.4
6.715
1.339
Ng2790
ppb
512.4
22.31
4.354
2203-1
ppb
483.3
9.182
1.9
Sel960
ppb
502.1
9.908
1.973
Zn2062
pob
510.1
15.28
2.995
Ba4934
ppb
513.2
7.886
1.537
Cr2677
PPb
506.5
8.25
1.629
Mn2576
ppb
504.1
5.34
1.059
2203-2
PPb
516.6
11.4
2.206
Snl899
ppb
495.5
5.998
1.21
512881
PPb
Q15540.
2786
17.92
Be3130
ppb
500.9
3.931
.7847
Cu3247
ppb
517.4
10.58
2.045
Mo2020
ppb
512.0
2.362
.4613
Sb2068
PPb
506.6
4.082
.8058
Sr4215
ppb
503.5
4.21
.8361
140
-------
Anaivsis Report
Averaaes
non 07-2:-' 06:51:53 AN oaae 47
Method: IRIANGL2 Sanple Name: ICB/CC8 Ooerator: DKH
Run Time: 07/28/97 05:30 Filename: 72797
Hode: CONC Type: 0 Corr. Factor: 1.00000
Lab ID.: Cust. Saol. ID.: Cust. ID.: 42298
Elans
Units
Avae
SDev
«SO
Eleis
Units
Avge
SDev
«SD
Eleis
Units
Avge
SDev
*RSD
Elens
Units
Avge
SDev
*RSD
Elens
Units
Avge
SDev
*RSD
Elems
Units
Avge
SDev
tRSD
Ag3280
ppb
Q-1.436
2.334
162.6
Ca3179
ppb
-1.252
1.066
85.17
Fe2714
ppb
4.477
18.26
407.9
Na3302
ppn
-.5711
.6733
117.9
1960-1
ppb
-6.157
4.87
79.09
Ti3349
ppb
.4658
.6758
145.1
A13082
ppb
31.64
6.803
21.5
Cd2265
ppb
.3500
.5685
162.4
X.7664
pp»
-.0993
.2481
249.7
Ni2316
ppb
1.305
1.03
78.9
1960-2
ppb
4.973
1.842
37.03
T11908
ppb
Q5.598
3.092
55.24
AS1890
ppb
-1.505
1.243
82.59
Ce4186
ppb
1.598
8.921
558.4
Li6707
ppb
.0741
.3774
509.2
P.2149
ppb
-2.770
3.507
126.6
Pb2203
ppb
1.371
.4604
33.58
V_2924
ppb
1.265
.9011
71.23
B.2496
ppb
-8.695
1.966
22.61
Co2286
ppb
.9275
.9962
107.4
MQ2790
ppb
10.26
4.721
46.02
2203-1
ppb
-6.219
4.532
72.88
Sel960
ppb
1.267
2.102
166
Zn2062
ppb
.6891
.6922
100.4
8a4934
Ppb
.4108
.5468
133.1
Cr2677
ppb
1.180
.6354
53.84
Nn2576
ppb
.3787
.4832
127.6
2203-2
ppb
5.161
2.644
51.24
Snl899
ppb
.6203
.7407
119.4
S12881
ppb
Q7602.
2229
29.32
8e3130
ppb
.5262
.4599
87.41
Cu3247
pob
.3997
1.215
304.1
Mo2020
ppb
1.054
.8494
80.58
Sb2068
ppb
1.589
2.535
159.5
Sr4215
ppb
.3199
.4821
150.7
141
-------
flnalvsis Recoct
Averaoes
«on 07-28-97 Oo:51:53 AM oaae 48
Method: TRIAN6L2 Saiole Name: 173-60-1A.10 X5 L Ooerator: DKH
Run Tiie: 07/28/97 05:40 Filenane: 72797
Mode: CONC Type: S Corr. Factor: 1.00000
Lab ID.: Cust. Siol. ID.: Cust. ID.: 42298
El ens
Units
Avge
SDev
«SD
AS1890
ppb
L.2084
1.945
933.5
8e3130
ppb
L.3095
.1015
32.78
Cd2265
ppb
31.34
.3945
1.259
Co2286
ppb
L.5172
1.233
238.4
Cr2677
PDD
10.43
1.187
11.39
Mn2576
DDb
21.71
.3006
1.385
El ess
Units
Avge
SDev
*RSD
Ni2316
ppb
36.11
2.128
5.894
Pb2203
ppb
6354.
30.81
.4849
Sb2068
ppb
L2.452
2.178
38.83
Sel960
ppb
10.04
.2737
2.725
142
-------
Analysis Reoort Averages
Mon 07-28-97 06:51:53 AM page 4<>
Method: TRIANGL2 Saiiple Mane: 173-60-2A X10 Ooerator: OKH
Run Tiae: 07/28/97 05:45 Filenaie: 72797
Moae: CONC Type: S Corr. Factor: 1.00000
Lao ID.: Cust. Snpl. ID.: Cust. ID.: 42298
Eleis
Units
Avge
SDev
tRSD
Asl890
ppo
L3.268
2.861
87.54
8e3130
ppb
L.2660
.0619
23.28
Cd2265
ppb
74.32
.4083
.5494
C02286
ppb
L.9368
.2731
29.15
Cr2677
ppb
20.62
.5663
2.746
Hn2576-
ppb
58.13
.6696
1.152
lisas
Units
Avge
SDe'v
*RSD
Ni2316
ppb
128.5
.5027
.3912
Pb2203 Sb2068
ppb ppb
15050. 8.192
633.1 2.037
4.207 24.87
S61960
ppb
23.53
2.691
11.44
143
-------
Analysis Report Averages
Mon 07-:a-97 06:51:53 AM oaoe 50
Method: TRIAN6L2 Sauole Na«e: 173-60-2A X10 OA Ooerator: OKH
Run Tiie: 07/28/97 05:52 Filename: 72797
Moae: COKC Type: S Corr. Factor: 1.00000
Lab 10.: Cust. Sipl. ID.: Cust. 10.: 42298
Elens
Units
Avge
SOev
*RSD
Asl890
ppb
L2.757
3.34
121.1
Be3130
ppb
L.2849
.0726
25.49
Cd2265
ppb
74.74
.418
.5592
Co2286
ppb
L.6759
.3714
54.94
Cr2677
ppb
20.46
.442
2.16
Mn2576
ppb
58.50
.5836
.9975
Eleis
Units
Avge
SDev
Ni2316
ppb
128.5
1.471
1.145
Pb2203 Sb2068
ppb ppb
14960. 6.059
353.6 .2953
2.364 4.874
Sel960
ppb
20.61
1.277
6.196
144
-------
Analysis Reoort Averages
Mon 07-28-97 06:51:55 AM page 51
Operator: DKH
Hetnod: TRIANGL2 Sample Naae: 173-60-3A X10
Run Tiae: 07/28/97 05:57 filenaie: 72797
Mooe: CONC Tyoe: S Corr. Factor: 1.00000
Lab ID.: Cust. SBol. ID.: Cust. 10.: 42298
fleas
Units
Avge
SDev
IRSD
AS1890
ppb
13.857
2.018
52.33
8e3130
ppb
L.2393
.0304
12.71
Cd2265
ppb
81.39
1.174
1.443
Co2286
ppb
L-.1085
.3899
359.2
Cr2677
ppb
20.95
.3946
1.883
Mn2576
ppb
121.2
1.731
1.428
Eleas
Units
Avge
SDev
«SD
N12316
ppb
74.28
.5238
.7051
Pb2203
ppb
16320.
221.4
1.357
Sb2068
ppb
10.79
1.145
10.62
Sel960
ppb
21.35
.8843
4.142
145
-------
Analysis Report Averages
Mon 07-28-97 06:51:53 AH cage 52
Operator: OKH
Method: TRIANGL2 Sasole Name: 173-60-12A X10
Run Tine: 07/28/97 06:02 Filenaie: 72797
Node: CQNC Type: S Corr. Factor: f 1.00000
Lab ID.: Cust. Siol. ID.: Ciist. ID.: 42298
Elenis
Units
Avge
SDev
«SD
Asl890
ppb
17.08
1.336
7.82
8e3130
POD
L.1591
.017
10.71
Cd2265
ppb
100.7
.6757
.6709
C02286
ppb
1.228
1.14
92.84
Cr2677
ppb
101.0
.6979
.6908
Hn2576
ppb
1531.
13.42
.8767
Elais Ni2316 Pb2203 Sb2068 Sel960
Units ppb ppb ppb ppb
Avge 143.8 19320. 14.13 44.08
SDev 1.297 384.5 .7837 .1058
WSD .9014 1.99 5.546 .24
146
-------
Anaivsis Reoort Averages
(ton 07-28-97 06:51:53 AM page 53
Ooeracor: DKH
Method: TRIAN6L2 Saiole Nane: 173-60-13A X10
Run Tiae: 07/28/97 06:08 Filena»e: 72797
Mode: CONC lyoe: S Corr. Factor: 1.00000
Lab ID.: Oust. Siol. 10.: Oust. ID.: 42298
El ens
Units
Avge
SDev
*RSD
Asl890
ppb
21.54
1.916
8.892
863130
ODD
I. 0000
.0296
322400
Cd2265
ppb
92.90
2.617
2.817
C02286
ppb
2.527
1.193
47.2
Cr2677
ppb
115.3
4.671
4.051
Mn2576
ppb
2091.
60.61
2.898
Eleis
Units
Avge
SOev
tRSD
Ni2316
ppb
96.96
3.42
3.527
Pb2203
ppb
18500.
570.9
3.086
S62068
ppb
11.04
4.146
37.54
Sel960
ppb
53.77
2.483
4.617
147
-------
Analysis Recoct
Averaaes
Hon 07-28-<>7 06:51:53 AN oaae 54
Method: TRIAN6L2 Sauole Nane: 173-60-14A X10 Operator: DXH
Run Tine: 07/28/97 06:13 Filenaie: 72797
Mode: CONC Type: S Corr. Factor: 1.00000
Lab ID.: Cust. Saipl. ID.: Cust. ID.: 42298
Ele«s
Units
Avge
SDev
tRSD
AS1890
ppb
23.32
1.518
6.51
8e3130
ppb
L.0352
.0168
47.79
Cd2265
ppb
95.94
.3955
.4122
Co2286
ppb
2.715
.2986
11
Cr2677
ppb
111.9
.8365
.7474
Mn2576
ppb
2187.
10.29
.4707
Eleis
Units
Avge
SDev
N12316
ppb
101.4
.5262
.5191
Pb2203 Sb2068
ppb ppb
19070. 11.21
141.8 2.172
.7434 19.37
Sel960
ppb
41.52
2.516
6.059
143
-------
Analysis Reoort
Averages
(ton 07-28-97 06:51:53 AH page 55
Method: TRIANGL2 Saiole Nane: 173-60-18 Operator: DXH
Run Tine: 07/28/97 06:19 Filenaie: 72797
Mode: CONC Tyoe: S Corr. Factor: 1.00000
Lab ID.: Cust. S»pl. ID.: Cust. 10.: 42298
Eleis
Units
Avge
SDev
*RSD
Asl890
ppb
L.2164
4.408
2037
8e3130
ppb
L.2049
.1438
70.19
Cd2265
ppb
5.910
.3796
6.423
Co2286
ppb
L-.5654
1.437
254.2
Cr2677
pob
25.39
2.004
7.892
Mn2576
ppb
101.4
1.664
1.641
Eleis
Units
Avge
SDev
tRSD
Ni2316
ppb
38.40
1.566
4.078
Pb2203
ppb
71.84
2.552
3.552
Sb2063 Sel960
ppb ppb
L2.266 168.6
4.159 .3696
183.6 .2192
149
-------
Analysis Reoort
Averages
lion 07-28-<57 06:51:53 AM oaae So
Method: TRIANGL2 Saiole iaie: ICV/CCV Operator: OKH
Run Tine: 07/28/97 06:24 Filenane: 72797
Mode: CONC Type: i Corr. Factor: 1.00000
Lap ID.: Cust. Siol. ID.: Cust. ID.: 42298
Ele»s
Units
Avge
SDev
*RSD
Elens
Units
Avge
SOev
«SO
Eleis
Units
Avge
SDev
*RSD
Elans
Units
Avge
SDev
*RSD
El ems
Units
Avge
SDev
*RSO
Eleas
Units
Avge
SDev
*RSD
Ag3280
PPP
512.3
.5843
.1141
Ca3179
ppb
0565.8
24.58
4.344
Fe2714
ppb
511.8
15.6
3.048
Na3302
DPI
5.192
.0699
1.346
1960-1
ppb
503.6
2.25
.4469
Ti3349
ppb
505.6
.8019
.1586
A13082
ODD
520.4
2.908
.5587
Cd2265
ppb
513.3
3.213
.626
K.7664
ppa
5.250
.2023
3.854
Hi2316
opb
517.2
1.306
.2526
1960-2
ppb
505.6
5.419
1.072
T11908
ppb
511.2
7.502
1.468
AS1890
ppb
510.6
5.642
1.105
Ce4186
ppb
515.3
5.61
1.089
116707
ppb
524.0
34.18
6.524
P.2149
ppb
511.1
10.9
2.133
Pb2203
ppb
511.1
9.509
1.86
V_2924
ppb
510.8
.7917
.155
8.2496
ppb
504.0
8.26
1.639
C02286
ppb
504.5
1.814
.3596
Mg2790
ppb
516.9
6.608
1.278
2203-1
ppb
489.6
6.076
1.241
Sel960
ppb
504.9
2.885
.5713
Zn2062
ppb
513.5
7.512
1.463
Ba4934
ppb
511.2
4.137
.8092
Cr2677
ppb
509.3
4.187
.8221
Mn2576
ppb
505.4
2.206
.4366
2203-2
ppb
521.9
11.9
2.28
Snl899
ppb
499.1
1.637
.3279
Si2881
ppb
Q40160.
17870
44.5
Be3130
opb
502.6
.4987
.0992
Cu3247
ppb
516.1
6.64
1.286
M02020
ppb
512.2
2.568
.5013
Sb2068
ppb
508.4
.871
.1713
Sr4215
ppb
501.7
2.385
.4753
150
-------
Analysis Reoort
Averaaes
Mon 07-28-97 06:51:53 AH page 57
Method: TRIANGL2 Sanole Na§e: IC8/CC8 Operator: DKH
Run Tine: 07/28/97 06:28 Filenaie: 72797
Mode: CONC Tyoe: 0 Corr. Factor: 1.00000
Lab ID.: Cust. Sad. ID.: Cust. ID.: 42298
El ens
Units
Avge
SOev
tRSD
El ens
Units
Avge
SDev
«SD
Ag3280 A13082
ppb ppb
.0670 28.80
.7264 8.478
1084 29.43
Ca3179 Cd2265
pob ppb
.0537 .1803
1.33 .2614
2477
Asl890
ppb
-.3197
1.781
557.2
Ce4186
ppb
04.150
8_2496
poo
-10.93
2.641
24.17
C02286
ppb
01.206
Ba4934 Be3130
ppb pob
.3013 .3420
.303 .1308
100.6 38.24
Cr2677 Cu3247
ppb ppb
1.313 .1535
217.7 79.24 97.69 725.2
Eleis
Units
Avge
SDev
*RSD
Elens
Units
Avge
SDev
*RSD
Eleios
Units
Avge
SDev
*RSD
Na3302 Ni2316
PP» ppb
-.0846 .7426
.2327 .9032
275.1 121.6
1960-1 1960-2
ppb ppb
568
ppb
29 07.151
2.506
35.04
Li6707
ppb
-.0900
.5376
597.2
P.2149
ppb
5.818
7.387 .
ill /
^2203
ppb
.5467
1.071
195.9
V.2924
ppb
1.621
1.07
66.01 _
MQ2790
ppb
12.26
8.817
71.93
2203-1 >
PPb/
/O311
X.167
1561
Sel960
ppb
-.7013
.8882
126.7
Zn2062
ppb
.7731
.2672,
Mn2576
ppb
.2439
.2596,
mV
/2203-2
ppb
.9850
3.927
398.7
Snl899
ppb
.3627
2.518
694.2
Si2881
pob
03765.^
^W3
65.95
Ho2020'
ppb/
/wn
/9454
231.9
Sb2068
ppb
2.403
4.677
194.6
Sr4215
ppb
.1583
.2111
133.3
_ — •
^^
-------
Analysis Report Averages
don 07-28-97 06:51:53 AM oaoe 58
Method: TRIANGL2 Saiole Name: IC8/CCB Operator: OKH
Run Tine: 07/28/97 06:34 Filenaie: 72797
Mode: CONC Type: 0 Corr. Factor: 1.00000
Lab ID.: Cust. Sioi. ID.: Cust. ID.: 42298
Eleis
Units
Avge
SDev
*RSD
Elems
Units
Avge
SDev
*RSD
Elesis
Units
Avge
SDev
*RSD
Eleis
Units
Avge
SDev
*RSD
Elens
Units
Avge
SDev
*RSD
Ag3280
ppb
-.9693
1.318
136
Ca3179
ppb — -
-.2651
2.73
1030
Fe2714
ppb
12.83
42.67
332.6
Na3302
ppn
-.1946
.4716
242.4
1960-1
ppb
-2.780
7.154
257.3
Ti3349/
ppb/
.4764
./331
/71.9
A13082
pob
31.27
19.74
63.12
Cd226^_
— pBB
^2421
.7051
291.2
K.7664
PP»
-.0149
.2163
1451
Ni2316
ppb
.9009
1.056
117.2
1960-2
ppb /
1.640
S.Jffl
X5
T11908
ppb
88.106
1.982
23.87
AS1890
ppb
-.9664
1.51
156.2
JMm~~
ppb
-1.798
6.204
345.1
Li6707
ppb
-.0238
.515
2161
PJ149
ppb
6.364
21.95
345 /
m.i
-------
Anaivsis Reoort
Averaaes
Non 07-23-97 06:51:53 AM oage 59
Method: TRIAN6L2 Samoie Na§e: IC8/CC8
Run riffle: 07/28/97 06:40 Filename: 72797
Ooerator: DKH
Hooe: CONC
Lab ID.
El ess
Units
Avge
SDev
*RSD
El ens
Units
Avge
SDev
*RSD
Eleis
Units
Avge
SDev
tRSD
Eleis
Units
Avge
SDev
*RSD
Eleis
Units
Avge
SDev
*RSD
Eleos
Units
Avge
SDev
*RSD
Tyoe: Q
Corr. Factor:
Cust. S«ol. ID.:
Ag3280
opb
0-1.887
1.79
94.89
Ca3179
ppb
-2.680
2.842
106
Fe2714
ppb
-12.68
36.64
289
Na3302
PP»
-.6113
.6117
100.1
1960-1
ppb
-4.135
9.514
230.1
T13349
ppb
-.2068
.7967
385.3
A13082
ppb
23.19
31.79
137.1
Cd2265
ppb
-.0615
.3282
534
K.7664
PP»
.0543
.2409
443.3
N12316
ppb
.0453
1.277
2822
1960-2
ppb
.6885
4.67
678.3
T11908
ppb
05.212
2.933
56.27
As 1890
ppb
1.014
1.258
124.1
C64186
ppb
.7859
6.681
850.2
Li6707
ppb
.1588
.5936
373.7
P.2149
ppb
-13.16
13.1
99.54
Pb2203
ppb
1.088
2.06
189.3
V.2924
ppb
-.0728
1.418
1947
8.2496
ODD
-17.30
3.047
17.62
Co2286
ppb
-.2361
1.586
671.8
Mg2790
ppb
-.2122
21.98
10360
2203-1
ppb
-5.772
7.047
122.1
Sel960
ppb
-.9177
.592
64.51
Zn2062
ppb
-.1360
.9578
704.3
1.00000
Cust. ID.: 42298
8a4934
ppb
-.1277
.3701
289.7
Cr2677
ppb
-.1315
2.053
1561
Hn2576
ppb
-.0438
.3008
686.2
2203-2
ppb
4.514
6.51
144.2
Snl899
ppb
-1.388
1.436
103.4
Si2881
ppb
0311.5
1769
567.9
8e3130
ppb
.1862
.1414
75.95
Cu3247
ppb
-1.308
2.631
201.1
Mo2020
ppb
.2634
1.151
437
Sb2068
ppb
-1.197
5.394
450.6
Sr4215
ppb
-.0365
.1619
443.3
-------
Analysis Reoort
Averaaes
Hon 07-28-97 06:51:53 AM paae 60
Nethoa: TRIANG12 Samole Name: ICSA8
Run Time: 07/28/97 06:45 Filename: 72797
Ooerator: DKH
Mode: CONC
Lab ID.
[lens
Units
Avge
SOev
*RSD
Eleas
Units
Avge
SDev
iRSD
Elens
Units
Avge
SOev
«SD
Ele»s
Units
Avge
SDev
*RSD
Elens
Units
Avge
SDev
USD
Elens
Units
Avge
SDev
tRSD
Tyoe: Q
Corr. Factor:
Cust. Siol. ID.:
Ag32SO
ppb
530.8
4.214
.7939
Ca3179
ppb
459300.
3283
.7147
Fe2714
ppb
173000.
256
.148
Na3302
PP»
5.482
.3159
5.763
1960-1
ppb
515.9
38.44
7.452
T13349
ppb
496.1
2.224
.4483
A13082
ppb
531800.
1344
.2528
Cd2265
ppb
468.2
.3802
.0812
K.7664
PP»
Q25.59
1.605
6.271
N12316
ppb
454.0
.2676
.0589
1960-2
ppb
510.0
26.58
5.211
T11908
ppb
508.3
10.13
1.993
AS1890
ppb
504.4
5.435
1.078
Ce4186
ppb
493.6
5.232
1.06
Li6707
ppb
575.1
43.38
7.543
P.2149
PPb
459.5
19.61
4.267
Pb2203
ppb
483.1
9.009
1.865
V_2924
PPb
495.6
2.506
.5056
B_2496
ppb
505.1
10.25
2.029
Co2286
ppb
465.5
.9373
.2014
Mg2790
ppb
536600.
2421
.4512
2203-1
ppb
504.8
13.17
2.609
Sel960
ppb
512.0
5.816
1.136
Zn2062
PPb
433.7
1.309
.3018
Cust.
Ba4934
ppb
509.9
4.925
.9657
Cr2677
PPb
483.3
.6849
.1417
Mn2576
ppb
454.7
.8408
.1849
2203-2
ppb
472.3
17.3
3.663
Snl899
ppb
479.7
3.872
.8072
S12881
ppb
Q10840.
943.6
8.709
1.00000
ID.: 42298
8e3130
poo
484.3
1.772
.3655
Cu3247
ppb
521.6
9.851
1.889
Mo2020
ppb
493.8
3.326
.6734
Sb2068
ppb
495.2
10.54
2.129
Sr4215
pub
0490.7
3.514
.716
154
-------
/Weight File: AB7SO.IDW
mple Volume: 100 mi-
Lac, Sample ID
0 STD BLK
1 STDl-0.2ug/L
2 STD2-0.5ug/L
3 3TD3-1.0ug/L
4 STD4=2.0ug/L
5 STD5=5.0ug/L
6 STD6-10.0ug/L
7 ICV=4.0ug/L
8 ICB
9 CHECK LO
10 42298 MB1
11 42298 MB1 D
12 42298 LCS1
13 42298 LCS1 D
14 173-60-12B
15 173-60-128 D
16 173-60-128 MS
17 173-60-126 MSD
18 173-60-12C
19 173-60-12C D
20 CCVl=6.0ug/L
21 CC81
22 173-60-12D
23 173-60-12D D
24 173-60-12E
25 173-60-12E D
26 173-60-13C
27 173-60-13C D
28 173-60-13D
29 173-60-13D D
30 173-60-13E
31 173-60-13E D
32 CCV2=6.0ug/L
33 CCB2
34 173-60-138
35 173-60-13B D
36 173-60-13B MS
37 173-60-138 MSD
38 173-60-14C
39 173-60-14C D
40 173-60-14D
41 173-60-14D D
42 173-60-14E
43 173-60-14E D
44 CCV3=6.0ug/L
45 CCB3
46 173-60-1C
47 173-60-1C D
48 173-60-1D
49 173-60-1D D
50 173-60-1E
51 173-60-1E D
52 173-60-2C
53 173-60-2C D
Analyst: RICHARDS
Nominal Weight: 1.0 g
Weight
Dilution
-H
•3-oob
-V
155
-------
Loc. Sample ID Weight Dilution
54 173-60-2D
55 173-60-2D D ., M, T fc /
-------
ement File: HG_.M£L
emen t: Hg2
int Data: Main+Suppl.
int: Calib. Curve
ma rks:
TANDARDS= 3-006-3
C- 3-006-4
Analyst: RICHARDS
Peak Storage: None
H
STRUMENT: 5100
velength: 253.7 Peak
gnal Type: AA
ad Time: 30.0
fnple Replicates: 1
andard Replicates: 1
Technique: MHS Version: 7.01
Slit: 0.7 Low
Signal Measurement: Peak Height (5)
Read Delay: 1.0 BOC Time: 2
AME:
ame Type: Air
idant Flow: 10.0 L/min
Flame Sensor: On
Fuel Flow: 2.0 L/min
_IBRATION:
Dlutions |
lib. B
andard
andard
andard
andard
andard
andard
lank
1
2
3
4
5
6
alibration
alibra
tion
1
JSTD
ISTD
ISTD
ISTD
ISTD
ISTD
ISTD
Units:
Type :
ID
BLK
1
2
3
4
5
6
Cone
0
0
1
2
5
10
.200
.500
.000
.000
.000
.000
i
i
i
i
i
i
|
|
i
t
i
ug/L Sample Units: ug/L
Linear
trix Check Calculations:
difference for Dupls: No
Recovery for Spike: No
Locations:
Locations:
Cone
157
-------
ID: STD 8LK
Seq. No.: 00022
A/S Pas.: --
Date: 07/21
'^eolicate 1
Peak Area (A-s): 0.001
Blank Corrected Pk Height (A): 0.000
Concentration (ug/L ): 0.007
Auto-zero performed.
Time: 12:51
Peak Height (A): 0.000
Hg2 ID: STDl=0.2ug/L
Seq. No.: 00023
A/S Pos.: --
Replicate 1
3eak Area (A-s): 0.184
Blank Corrected Pk Height (A): 0.009
Concentration (ug/L ): 0.213
Standard number 1 applied. [0.200]
Correlation coefficient: 1.00000
Time: 12:53
Peak Height (A): 0.009
Slope: 0.0426
Date: 07/21/97
Hg2 ID: STD2-0.5ug/L
Seq. No.: 00024
A/S Pos.: --
Sample abs. is greater than that of the largest standard.
Replicate 1 Time: 12:54
3eak Area (A-s): 0.464 Peak Height (A): 0.021
Uank Corrected Pk Height (A): 0.021
Concentration (ug/L ): 0.485
Standard number 2 applied. [0.500]
Correlation coefficient: 0.99962
Slope: 0.0415
Date: 07/21/9'
ig2 ID: STD3=1.0ug/L
Seq. No.: 00025
A/S Pos.: —
'-ample abs. is greater than that of the largest standard.
eak. Area (A-s): 0.895 Peak Height (A): 0.042
;lank Corrected Pk Height (A): 0.042
:oncentration (ug/L ): 1.000
;tandard number 3 applied. [1.000]
•orrelation coefficient: 0.99995
Slope: 0.0415
Date: 07/21/97
ID: STD4-2.0ug/L
Seq. No.: 00026
A/S Pos.: --
-ample abs. is greater than that of the largest standard.
eplicate 1 Time: 12:57
]eak Area (A-s): 1.836 Peak Height (A): 0.082
lank Corrected Pk Height (A): 0.082
oncentration (ug/L ): 1.986
tandard number 4 applied. [2.000]
orrelation coefficient: 0.99998
Slope: 0.0413
Date: 07/21/9^
158
-------
12 ID: STD5-5.0ug/L Seq. No.: 00027 A/S Pos.: -- Data: 07/21/97
,mple abs. is greater than that of the largest standard.
iplicate 1 Time: 12:58
ak Area (A-s): 4.633 Peak Height (A): 0.20S
ank Corrected Pk Height (A): 0.208
incentration (ug/L ): 5.047
.andard number 5 applied. [5.000]
rrelation coefficient: 0.99998 Slope: 0.0416
2 ID: STD6=10.0ug/L Seq. No.: 00028 A/S Pos.: — Date: 07/21/97
mple abs. is greater than that of the largest standard.
plicate 1 Time: 12:59
ak Area (A-s): 9.190 Peak Height (A): 0.408
ank Corrected Pk Height (A): 0.408
ncentration (ug/L ): 9.804
andard number 6 applied. [10.000]
rrelation coefficient: 0.99993 Slope: 0.0410
159
-------
Element File: HG_.MEL
Date: 07/21/97
Data File: AB78O.DAT
Technique: MHS
Remark 1: STANDARDS= 3-006-3
Remark 2: QC= 3-006-4
Element: Hg2
Time: 13:00
ID/Wt File: AB780.IDW
Calib. Type: Linear
Wavelength:
Slit: 0.7 L
Lamp Current
Energy: 73
53.7
H
Display Calibration - C:\ffl_USER\flfl.FILES\ELEHEHT\H6_.HEL
0.408i
Linear
Corn. Coef.: B.99993
Slope: O.B41Q
Concentration
18.
160
-------
ement File; HG_.MEL
te: 07/21/97
ta File: AB780.DAT
chnique: MHS
mark 1: STANDARDS- 3-006-3
mark 2: QC= 3-006-4
Element: Hg2
Time: 13:02
ID/Wt File: AB780.IDW
Calib. Type: Linear
Wavelength: 253.7
Slit: 0.7 L
Lamp Current: 0
Energy: 73
ID: ICV=4.0ug/L
Seq. No
plicate 1
ak Area (A-s): 3.511
ank Corrected Pk Height (A): 0.155
ncentration (ug/L ): 3.780
00029
A/S Pos.: --
Date: 07/21/97
Time: 13:03
Peak Height (A): 0.155
ID: ICB
Seq. No.
olicate 1
ak Area (A-s): -0.006
ank Corrected Pk Height (A): -0.000
ncentration (ug/L ): -0.002
00030
A/S Pos.: --
Date: 07/21/97
Time: 13:05
Peak Height (A):
-0.000
ID: CHECK LO
Seq. No.: 00031
olicate 1
ak Area (A-s): 0.174
ank Corrected Pk Height (A): 0.008
-icentration (ug/L ): 0.188
A/S Pos.: —
Date: 07/21/9:
Time: 13:06
Peak Height (A): 0.008
ID: 42298 MB1
Seq. No.: 00032
Dlicate 1
ak Area (A-s): 0.008
ank Corrected Pk Height (A): 0.001
icentration (ug/L ): 0.015
A/S Pos.: —
Date: 07/21/97
Time: 13:07
Peak Height (A): 0.001
ID: 42298 MB1 D
Seq. No,
>licate 1
ik Area (A-s): 0.003
ink Corrected Pk Height (A): 0.001
icentration (ug/L ): 0.024
00033
A/S Pos.: —
Date: 07/21/97
Time: 13:08
Peak Height (A): 0.001
: ID: 42298 LCS1
>licate 1
.k Area (A-s) : 5. 157
ink Corrected Pk Height (A)
icentration (ug/L ): 6.046
Seq. No.: 00034
0.248
A/S Pos.: --
Date: 07/21/97
Time: 13:09
Peak Height (A): 0.248
ID: 42298 LCS1 D
Seq. No.: 00035
A/S Pos.: --
Date: 07/21/97
161
-------
3eak Area (A-s): 5.097
Blank Corrected Pk Height (A): 0.241
Concentration (ug/L ): 5.882
Time: 13:10
Peak Height (A?: 0.241
ID: 173-60-126
Seq. No.: 00036
Replicate 1
3eak Area (A-s): 0.051
ilank Corrected Pk Height (A): 0.002
;oncentration (ug/L ): 0.056
A/S Pos. : —
Date: 07/21/9"
Time: 13:16
Peak Height (A): 0.002
ID: 173-60-128 D
Seq. No.: 00037
A/S Pos.: —
Date: 07/21/97
.eplicate 1
:eak Area (A-s): 0.064
lank Corrected Pk Height (A): 0.003
oncentration (ug/L ): 0.069
Time: 13:17
Peak Height (A): 0.003
92
ID: 173-60-12B MS
Seq. No.: 00038
eplicate 1
eak Area (A-s): 3.683
lank Corrected Pk Height (A): 0.167
oncentration (ug/L ): 4.069
A/S Pos.: --
Date: 07/21/97
Time: 13:18
Peak Height (A): 0.167
ID: 173-60-12B MSD
Seq. No.: 00039
eplicate 1
eak Area (A-s): 3.361
lank Corrected Pk Height (A): 0.155
oncentration (ug/L ): 3.787
A/S Pos.: —
Date: 07/21/97
Time: 13:19
Peak Height (A): 0.155
ID: 173-60-12C
Seq. No.: 00040
eplicate 1
eak Area (A-s): 0.292
lank Corrected Pk Height (A): 0.013
oncentration (ug/L ): 0.311
A/S Pos.: --
Time: 13:21
Peak Height (A):'0.013
Date: 07/21/97
g2 ID: 173-60-12C D
Seq. No.: 00041
eplicate 1
eak Area (A-s): 0.280
lank Corrected Pk Height (A): 0.012
oncentration (ug/L ): 0.301
A/S Pos.: --
Time: 13:22
Peak Height (A): 0.012
Date: 07/21/9'
g2 ID: CCVl-6.0ug/L
Seq. No.
00042
A/S Pos.: --
eplicate 1
sak Area (A-s): 4.930
lank Corrected Pk Height (A): 0.220
Time: 13:23
Peak Height (A): 0.220
Date: 07/21/97
162
-------
-icentration (ug./L ): 5.356
: ID: CCB1 Seq. No.: 00043 A/S Pos.: — Date: 07/21/9^
Dlicate 1 Time: 13:24
ak Area (A-s): -0.008 Peak Height (A): O.OOO
ank Corrected Pk Height (A): 0.000
-icentration (ug/L ): 0.000
2 ID: 173-60-12D Seq. No.: 00044 A/S Pos.: — Date: 07/21/97
Dlicate 1 Time: 13:25
sk Area (A-s): 0.040 Peak Height (A): 0.002
ank Corrected Pk Height (A): 0.002
•icentration (ug/L ): 0.039
I ID: 173-60-12D D Seq. No.: 00045 A/S Pos.: — Date: 07/21/97
>licate 1 Time: 13:26
ik Area (A-s): 0.039 Peak Height (A): 0.002
jnk Corrected Pk Height (A): 0.002
icentration (ug/L ): 0.042
! ID: 173-60-12E Seq. No.: 00046 A/S Pos.: — Date: 07/21/97
>licate 1 Time: 13:28
ik Area (A-s): 0.001 Peak Height (A): -0.000
ink Corrected Pk Height (A): -0.000
icentration (ug/L ): -0.005
: ID: 173-60-12E D Seq. No.: 00047 A/S Pos.: — Date: 07/21/97
ilicate 1 Time: 13:29
.k Area (A-s): -0.004 Peak Height (A): -0.000
mk Corrected Pk Height (A): -0.000
icentration (ug/L ): -O.OO2
ID: 173-60-13C Seq. No.: 00048 A/S Pos.: -- Date: 07/21/9^
• licate 1 Time: 13:32
k Area (A-s): -O.015 PeaK Height (A): -0.001
nk Corrected Pk Height (A): -0.001
centration (ug/L ): -0.015
Seq. No.: 00049
ID: 173-60-13C D
licate 1
k Area (A-s): -0.017
nk Corrected Pk Height (A): -0.001
centration (ug/L ): -0.022
A/S Pos.: --
Date: 07/21/9'
Time: 13:33
Peak Height (A): -0.001
163
-------
Hai
ID: 173-60-13D
Seq. No.: 00050
A/S Pos
Date: 07/21/9"
^eplicata 1
^eak Area (A-s): 0.008
Blank Corrected Pk Height (A): 0.000
Concentration (ug/L ): 0.007
Time: 15:35
Peak Height (A): 0.000
ID: 173-60-13D D
Seq. No.: 00051
Replicate i
^eak Area (A-s): 0.008
31ank Corrected Pk Height (A): 0.000
Concentration (ug/L ): 0.007
A/S Pos.: --
Time: 13:36
Peak Height (A): 0.000
Date: 07/21/9:
ID: 173-60-13E
Seq. No.: 00052
Replicate 1
3eak Area (A-s): -0.007
Blank Corrected Pk Height (A): 0.000
Concentration (ug/L ): 0.002
A/S Pos.: --
Date: 07/21/97
Time: 13:37
Peak Height (A): 0.000
ID: 173-60-13E D Seq. No
Replicate 1
Deak Area (A-s): -0.008
Blank Corrected Pk Height (A): -0.000
Concentration (ug/L ): -0.002
00053
A/S Pos.: --
Date: 07/21/97
Time: 13:38
Peak Height (A): -0.000
ID: CCV2=6.0ug/L
Seq. No.: 00054
Replicate 1
Jeak Area (A-s): 4.845
Uank Corrected Pk Height (A): 0.214
Concentration (ug/L ): 5.219
A/S Pos.: --
Date: 07/21/97
Time: 13:40
Peak Height (A): 0.214
ID: CCB2
Seq. No.: OO055
Replicate 1
Jeak Area (A-s): 0.003
ilank Corrected Pk Height (A): 0.000
;oncentration (ug/L ): 0.000
A/S Pos'. : --
Date: 07/21/9'
Time: 13:41
Peak Height (A): O.OOO
ID: 173-60-13B
Seq. No.: 00056
.eplicate 1
'eak Area (A-s): 0.127
lank Corrected Pk Height (A): 0.005
:oncentration (ug/L ): 0.127
A/S Pos.: --
Date: 07/21/97
Time: 13:43
Peak Height (A): 0.005
ID: 173-60-13B D
Seq. No.: 00057
A/S Pos.: --
Date: 07/21/97
164
-------
olicate 1
ak Area (A-s): 0.126
ank Corrected Pk Height (A): 0.006
-icentration (ug/L ): 0.137
Time: 13:44
Peak Height (A): 0.006
ID: 173-60-13B MS
Seq. No.: 00058
plicate 1
ak Area (A-s): 4.530
ank Corrected Pk Height (A): 0.197
-icentration (ug/L ): 4.808
A/S Pos.:
Time: 13:45
Peak Height (A): 0.197
Date: 07/21/97
ID: 173-60-13B MSD
Seq. No.: 00059
A/S Pos.: --
plicate 1
ik Area (A-s): 4.730
ank Corrected Pk Height (A): 0.210
•icentration (ug/L ): 5.116
Time: 13:46
Peak Height (A): 0.210
Date: 07/21/97
ID: 173-60-14C
Seq. No.
>licate i
ik Area (A-s): 0.016
ink Corrected Pk Height (A): O.OO1
icentration (ug/L ): 0.015
00060
A/S Pos.: —
Date: 07/21/9"
Time: 13:47
Peak Height (A): 0.001
ID: 173-60-14C D
Seq. No.: 00061
>licate 1
ik Area (A-s'): 0.000
ink Corrected Pk Height (A): 0.000
icentration (ug/L ): 0.000
A/S Pos.: --
Date: 07/21/97
Time: 13:49
Peak Height (A): 0.000
ID: 173-60-14D
Seq. No.: 00062
>licate 1
,k Area (A-s): 0.050
,nk Corrected Pk Height (A): 0.002
-centration (ug/L ): 0.054
A/S Pos.: —
Date: 07/21/9-
Time: 13:50
Peak Height (A):"0.002
ID: 173-60-140 D
Seq. No.: 00063
A/S Pos.: --
Date: 07/21/9:
•licate 1
k Area (A-s): 0.051
nk Corrected Pk Height (A): 0.002
centration (ug/L ): 0.054
Time: 13:51
Peak Height (A): 0.002
ID: 173-60-14E
Seq. No.: 00064
licate 1
k Area (A-s): 0.005
nk Corrected Pk Height (A): 0.000
A/S Pos.: --
Date: 07/21/9'
Time: 13:52
Peak Height (A): 0.000
165
-------
Concentration (ug/L ): 0.002
Ha:
ID: 175-60-14E D
Seq. No.: O0065
Replicate 1
Peak Area (A-s): 0.004
Blank Corrected Pk Height (A): 0.000
Concentration (ug/L ): 0.005
A/S Pos.: --
Date: 07/21/9'
Time: 13:53
Peak Height (A): 0.000
Hg2 ID: CCV3=6.Oug/L
Seq. No.: 00066
Replicate 1
Peak Area (A-s): 4.891
Blank Corrected Pk Height (A): 0.213
Concentration (ug/L ): 5.202
A/S Pos.: --
Date: 07/21/9'
Time: 13:54
Peak Height (A): 0.213
ID: CC83
Seq. No.: 00067
Replicate 1
^eak Area (A-s): 0.002
Slank Corrected Pk Height (A): 0.000
Concentration (ug/L ): 0.005
A/S Pos.: --
Date: 07/21/9:
Time: 13:55
Peak Height (A): 0.000
Hg2
ID: 173-60-1C
Seq. No.: OO068
Replicate 1
3eak Area (A-s): -0.002
Blank Corrected Pk Height (A): 0.000
Concentration (ug/L ): 0.000
A/S Pos.: --
Date: 07/21/97
Time: 13:56
Peak Height (A): 0.000
ID: 173-60-1C D
Seq. No.: 00069
Reolicate 1
3eak Area (A-s): -0.006
Blank Corrected Pk Height (A): -0.000
Concentration (ug/L ): -0.002
A/S Pos.: --
Date: 07/21/97
Time: 13:58
Peak Height (A): -0.000
ID: 173-60-1D
Seq. No.
Replicate 1
3eak Area (A-s): 0.277
Uank Corrected Pk Height (A): 0.012
Concentration (ug/L ): 0.289
00070
A/S Pos.: —
Date: 07/21/9'
Time: 13:59
Peak Height (A): 0.012
192
ID: 173-60-1D D
Seq. No.: 00071
Replicate 1
Jeak Area (A-s): 0.289
Jlank Corrected Pk Height (A): 0.013
:oncentration (ug/L ): 0.308
A/S Pos.: --
Date: 07/21/9'
Time: 14:00
Peak Height (A): 0.013
166
-------
ID: 173-60-1E
Seq. No,
OOOT:
A/S Pos.: --
Date: 07/21/9"
•plicate 1
•ak Area ( A-s ) : 0.019
ank Corrected Pk Height (A): 0.001
mcentration (ug/L ): 0.020
Time: 14:01
Peak Height (A): 0.001
ID: 173-60-1E D
Seq. No.: 00073
iplicate 1
ak Area (A-s): 0.020
ank Corrected Pk Height (A): 0.001
ncentration (ug/L ): 0.027
A/'S Pos. : —
Time: 14:02
Peak Height (A): 0.001
Date: 07/21/97
ID: 173-60-2C
Seq. No.: 00074
plicate 1
ak Area (A-s) : -0.013
ank Corrected Pk Height (A): -0.001
ncentration (ug/L ): -0.015
A/S Pos.: --
Time: 14:03
Peak Height (A):
-0.001
Date: 07/21/9'
Seq. No.: 00075
2 ID: 173-60-2C D
plicate 1
ak Area (A-s): -0.011
ank Corrected Pk Height (A): -0.000
ncentration (ug/L ): -0.007
A/S Pos.: —
Time: 14:04
Peak Height (A): -0.000
Date: 07/21/97
ID: 173-60-2D
Seq. No.: 00076
plicate 1
ak Area (A-s) : 0.346
ank Corrected Pk Height (A): 0.015
ncentration (ug/L ): 0.360
A/S Pos.: —
Time: 14:05
Peak Height (A): 0.015
Date: 07/21/97
ID: 173-60-2D D
Seq. No,
olicate 1
ak Area (A-s): 0.337
ank Corrected Pk Height (A): 0.015
ncentration (ug/L ): 0.362
00077
A/S Pos.: --
Time: 14:06
Peak Height (A): 0.015
Date: 07/21/97
ID: CCV4=6.0ug/L
Seq. No.: 00078
plicate 1
ak Area (A-s): 4.871
ank Corrected Pk Height (A): 0.218
-icentration (ug/L ): 5.317
A/S Pos.: —
Time: 14:07
Peak Height (A): 0.218
Date: 07/21/97
ID: CCB4
Seq. No.: 00079 A/S Pos.: -- Date: 07/21/9'
167
-------
Replicate 1
Peak Area (A-s): -0.015
Blank Corrected Pk Height (A):
Concentration (ug/L ): -0.017
-0.001
Time: 14:10
Peak Height (A)
-0.001
Ha2 ID: 173-60-148
Seq. No.: 00080
Reolicate 1
Peak Area (A-s): 0.114
Blank Corrected Pk Height (A): 0.005
Concentration (ug/L ): 0.125
A/S Pos.: --
Time: 14:11
Peak Height (A): 0.005
Date: 07/21/9"
ID: 173-60-14B D
Seq. No.: 00081
A/S Pos.: --
Date: 07/21/9'
Replicate 1
Peak Area (A-s): 0.116
Blank Corrected Pk Height (A): 0.005
Concentration (ug/L ): 0.130
Time: 14:12
Peak Height (A): 0.005
ID: 173-60-14B MS
Seq. No.: 00082
^eolicate 1
^eak Area (A-s): 4.669
31ank Corrected Pk Height (A): 0.208
Concentration (ug/L ): 5.077
A/S Pos. : —
Time: 14:13
Peak Height (A): 0.208
Date: 07/21/97
ID: 173-60-14B MSD
Seq. No.: 00083
Replicate 1
:>eak Area (A-s): 4.734
Blank Corrected Pk Height (A): 0.212
Concentration (ug/L ): 5.170
A/S Pos.: --
Time: 14:14
Peak Height (A): 0.212
Date: 07/21/9'
ID: 173-60-2E
Seq. No.: 00084
A/S Pos. : —
Replicate 1
3eak Area (A-s): 0.032
ilank Corrected Pk Height (A): 0.002
Concentration (ug/L ): 0.042
Time: 14:15
Peak Height (A):' 0.002
Date: 07/21/97
ID: 173-60-2E D
Seq. No.: OO085
Replicate 1
3eak Area (A-s): 0.018
ilank Corrected Pk Height (A): 0.001
:oncentration (ug/L ): 0.020
A/S Pos.: —
Time: 14:16
Peak Height (A): 0.001
Date: 07/21/97
•92
ID: 173-60-3C
Seq. No.: 00086
.eplicate 1
eak Area (A-s): -0.016
lank Corrected Pk Height (A): -0.001
A/S Pos.: --
Date: 07/21/97
Time: 14:18
Peak Height (A): -0.001
168
-------
-icentration (.ug/L ): -0.015
ID: 173-60-3C D
Seq. No.: 00087
olicate 1
ak Area (A-s): -0.019
ank Corrected Pk Height (A): -0.001
-icentration (ug/L ): -0.012
A/S Pos.: —
Time: 14:19
Peak Height (A):
-0.001
Date: 07/21/97
ID: 173-60-3D
Seq. No,
plicate 1
ak Area (A-s): 0.552
ank Corrected Pk Height (A): 0.024
•icentration (ug/L ): 0.595
00088
A/S Pos.: --
Time: 14:21
Peak Height (A): 0.024
Date: 07/21/97
ID: 173-60-3D D
Seq. No.: 00089
ilicate 1
ik Area (A-s): 0.562
ink Corrected Pk Height (A): 0.024
•icentration (ug/L ): 0.582
A/S Pos. : --
Time: 14:22
Peak Height (A): 0.024
Date: 07/21/9:
ID: CCV5=6.0ug/L
Seq. No,
>licate 1
ik Area (A-s): 5.126
jnk Corrected Pk Height (A): 0.222
icentration (ug/L ): 5.424
00090
A/S Pos.: --
Time: 14:23
Peak Height (A): 0.222
Date: 07/21/97
ID: CCB5
Seq. No,
>licate 1
ik Area (A-s): -0.011
ink Corrected Pk Height (A): -0.000
icentration (ug/L ): -0.005
00091
A/S Pos.: --
Time: 14:24
Peak Height (A):
-0.000
Date: 07/21/97
ID: 173-60-3E
Seq. No.: 00092
>licate 1
,k Area (A-s) : 0.006
,nk Corrected Pk Height (A): 0.001
icentration (ug/L ): 0.012
A/S Pos.: --
Time: 14:25
Peak Height (A): 0.001
Date: 07/21/97
ID: 173-60-3E D
Seq. No.: 00093
licate 1
k Area (A-s): -0.001
nk Corrected Pk Height (A): 0.000
centration (ug/L ): 0.007
A/S Pos.: --
Time: 14:26
Peak Height (A): 0.000
Date: 07/21/97
169
-------
Hg2 ID: CCV6=6.Oug/L Seq. No.: 000=54 A/S Pos. : -- Date: 07/21/9'
Replicate 1 Time: 14:27
Peak Area (A-s): 4.867 Peak Height (A): 0.2O8
Blank Corrected Pk Height (A): 0.208
Concentration (ug/L ): 5.070
Hg2 ID: CCB6 Seq. No.: 00095 A/S Pos.: -- Date: 07/21/9:
Replicate 1 Time: 14:28
Peak Area (A-s): -0.014 Peak Height (A): -0.001
Blank Corrected Pk Height (A): -0.001
Concentration (ug/L ): -0.017
170
-------
/Weioht rile: A6785.IDW
•nole Volume: 100 mL
Lac.
Samole ID
0
1
-n
o
4
5
o
7
5
g
10
11
12
13
14
15
16
17
13
19
20
21
22
23
24
25
26
27
28
29
30
31
32
33
34
3 5
36
37
33
39
40
41
42
43
44
45
46
47
48
49
50
51
52
53
STQ BLK
ST01=0.2ug/L \
3102=0 . 5ug/L
STD3-1 .Oug/L
STD4=2.0ug/L
STD5=5.0ug/L
5TDo= 10. Oug/L
ICV = 4.0ug/L
ICS
CHECK LO
422°S M82
42293 MB2 0
42293 LCS2
'42298 LCS2 D
173-60-iB
173-60-1B 0
173-60-IB MS
173-60-IB MSD
174-97-3/13
174-97-3/13 D
CCV 1-6. Oug/L —
;" CCB1
173-60-4AB
173-60-4AB 0
173-60-4C
173-60-4C D
173-60-4D
173-60-40 D
174-97-9/19
174-97-9/19 D
173-60-2B
173-60-2B D
CCV2-6 . Oug/L • —
CCS 2
173-60-2B MS
l"73-60-2B MS D
173-60-5&^ift&
1 7 3 - 6 0 - 5^^DC^,-J(
173-60-5C
173-60-5C D
173-60-50
173-60-50 D
174-97-10/20
174-97-10/20 D
CCV3-6.0ug/L —
CCB3
173-60-llAB
173-60-llAB D
173-60-11A ^.
173/^-60-1 1A 0
173-60-110
173-60-110 D
173-60-3B
173-60-3B D
Anal/st: RICHARDS
Nominal Weiaht: 1.0
"
Weioht
Dilution
3,
a.
171
-------
Loc. Sample ID Weight Dilution
54 173-60-3B MS
55 173-60-38 MS D ^^ -7
56 CCV4 = 6.0ug/L _ ;S-DO Jr - U
60 L73-60-6AC
61 173-60-6AC D
62 173-60-6D
63 173-60-6D D
64 173-60-7
65 173-60-7 D
66 174-97-4/13
67 174-97-4/13 D
68 CCV5-6 . Oug/'L
69 'CCB5
70 42298 M83
71 42298 MB3 D
72 422QS LCS3
73 42298 LCS3 D
74 174-97-6/15
75 174-97-6/15 D
76 L "7^-^7-6/15
77 :' 174-97-6/15 MS
78 174-97-6/15 MSD
79 174-97-1/11
80 174-97-1/11 D
81 CCVl-6.0ug./L
32 CC61
83 174-97-2/3
84 174-97-2/3 D
85 174-97-5/14
86 174-97-5/14 D
87 174-97-7/16
88 174-97-7/16 D
89 173-60-4DE
90 173-60-4DE D
91 173-60-5DE
92 173-60-5DE D
93 CCV2-6.0ug/L
94 CCB2
95 '173-60-6DE
96 173-60-6DE D
97 173-60-6DE MS
98 173-60-6DE MSD
99 173-60-llDE
100 173-60-llDE D
101 173-60-6B
102 173-60-6B D
103 CCV3-6.0ug/L
104 CCB3
172
-------
iment File: HG_.MEL
imenC: Hg2
nt Data: Main+Suppl.
.nt: Calib. Curve
larks :
'ANDARDS- 3-008-1
:= 3-008-2
Analyst: RICHARDS
Peak Storage: None
JTRUhENT: 5100
'elength: 253.7 Peak
inal Type: AA
id Time: 30.0
tple Replicates: 1
m'dard Replicates: 1
Technique: MHS Version: 7.01
Slit: 0.7 Low
Signal Measurement: Peak Height (5)
Read Delay: 1,0 BOC Time: 2
iME:
ime Type:
.dant Fl.ow
.IBRATION:
)lu tions
. i b . Blank
indard 1
indard 2
indard. Z
jndard" 4
indard 5
indard 6
ilibration
jlibration
Air Flame Sensor: On
: 10.0 L/min Fuel Flow: 2.0 L/min
i ID ! Cone
i t
i
1 O T Pi Q 1 I/ -. _
ibiDBLK. — —
ISTD i 0.200
iSTD 2 0.500
ISTD 3 i.ooo
ISTD 4 2.000
ISTD 5 5.000
ISTD 6 10.000
Units: ug/L Sample Units: ug/L
Type: Linear
:rix Check Calculations:
>ifference for Dupls: No
Recovery for Spike: No
Locations:
Locations:
Cone:
173
-------
Element File: HG_.MEL
Data: 07/29/97
:>ata File: AB785.DAT
Technique: MHS
Remark 1: STANDARDS^ 3-008-1
Remark 2: QC- 3-008-2
Element: Hg2
Time: 12:22
ID/Wt File: AB785.IDW
Calib. Type: Linear
Wavelength: 253
Slit: 0.7 L
Lamp Current: 0
Energy: 73
Ha2
ID: STD BLK
Seq. No.: 00003
Replicate 1
3eak Area (A-s): -0.003
Blank Corrected Pk Height (A): 0.000
Concentration (ug/L ): 0.003
^uto-zero performed.
A/S Pos.: --
Time: 12:24
Peak Height (A): 0.000
Date: 07/29/97
ID: STDl=0.2ug/L
Seq. No,
Replicate 1
3eak Area (A-s): 0.182
Blank Corrected Pk Height (A): 0.008
:oncentration (ug/L ): 0.219
Standard number 1 applied. [0.200]
:orrelation coefficient: 1.00000
00004
A/S Pos.: —
Time: 12:25
Peak Height (A): 0.008
Slope: 0.0401
Date: 07/29/9"
ID: STD2=0.5ug/L
Seq. No.: 00005
A/S Pos.: —
Sample abs. is greater than that of the largest standard.
'.eplicate 1 Time: 12:26
3eak Area (A-s): 0.447 Peak Height (A): 0.018
lank Corrected Pk Height (A): 0.018
Concentration (ug/L ): 0.460
:tandard number 2 applied. [0.500]
Correlation coefficient: 0.99717
Slope: 0.0374
Date: 07/29/9'
-------
nk Corrected Pk Height (A): O.O"715
icentration iug/L ): 2.157
nda-d number 4 applied. [2.000J
relation coefficient: 0.99848 Slope: 0.0390
ID: STD5-5.0ug/L Seq. No.: 00008 A/S Pos.: — Date: 07/29/17
pie abs. is greater than that of the largest standard.
licate 1 Time: 12:30
k Area (A-s»: 4.655 Peak Height (A): 0.202
nk Corrected Pk Height (A): 0.202
centration (ug/L ): 5.171
ndard number 5 applied. [5.000]
relation coefficient: 0.99965 Slope: 0.0401
ID: STD6 = 10.0ug/L Seq. No.: 00009 A/S Pos.: -- Date: 07/29/9"'
pie abs. is greater than that of the largest standard.
licate 1 Time: 12:31
k Area ('A-s ) : . 9. 052 Peak Height (A): 0.380
nk Corrected Pk Height (A): 0.380
centration (ug/L ): 9.459
ndard number 6 applied. [10.000]
relation coefficient: 0.99941 Slope: 0.0385
173
-------
-Ilement File: HG_.MEL Element: Hg2
)ate: 07/2G/^7 Time: 12:32
)ata File: A87S5.DAT ID/Wt File: AB785.IDW
"echnique: MHS Calib. Type: Linear
Remark 1: STANDARDS- 3-008-1
Remark 2: QC- 3-008-2
Wavelength: 253.7
Slit: 0.7 L
Lamp Current: 0
Energy: 73
H
Display Calibration - C:\flfl.USER\flfl.FILES\ELEHEHT\H6,.HEL
0.3801
Linear
Corn. Coef.: B.99941
Slope; 0.0385
Concentration
18.888
176
-------
2 m e n D File: HG_.fv!EL
ze: 07/29-97
ta File: AB7S5.DAT
zhnique: MHS
nark 1: STANDARDS: 3-008-1
nark 2: QC- 3-008-2
Element: Hg2
Time: 12:35
ID/Wt File: AB785.IDW
Calib. Type: Linear
Wavelength: 253.7
Slit: 0.7 L
Lamp Current: 0
Energy: 73
2 ID: ICV=4.0ug/L Seq. No
plicate 1
ak Area (A-s): 3.632
ank Corrected Pk Height (A): 0.161
-icentraticn (ug/'L ): 4.172
00010
A/S Pos.: --
Date: 07/29/97
Time: 12:35
Peak Height (A): 0.161
ID: ICB
Seq. No.: 00011
plicate 1
ik Area (A-s) : 0.018
ank Corrected Pk Height (A): 0.000
•icentration (ug/L ): 0.005
A/S Pos
Date: 07/29/9'
Time: 12:36
Peak Height (A): 0.000
ID: CHECK LO
Seq. No.: 00012
slicate 1
ik Area (A-s) : 0.191
ink Corrected Pk Height (A): 0.008
-icentration (ug/L ): 0.211
A/S Pos
Date: 07/29/9"
Time: 12:38
Peak Height (A): 0.008
ID: 42298 M82
Seq. No.: 00013
)licate 1
ik Area (A-s) : 0.030
ink Corrected Pk Height (A): 0.001
•icentration (ug/L ): 0.029
A/S Pos.: --
Date: 07/29/9'
Time: 12:40
Peak Height (A): 0.001
ID: 42298 MB2 D
Seq. No.: 00014
jlicate 1
jk Area (A-s ) : 0.019
ink Corrected Pk Height (A): 0.001
-icentration (ug/L ): 0.018
A/S Pos'. : --
Date: 07/29/9"
Time: 12:41
Peak Height (A): 0.001
ID: 42298 LCS2
Seq. No.: 00015
jlicate 1
ik Area (A-s): 4.423
ink Corrected Pk Height (A): 0.190
icentration (ug/L ): 4.928
A/S Pos.: --
Date: 07/29/9^
Time: 12:42
Peak Height (A): 0.190
ID: 42298 LCS2 D
Seq. No.: 00016
A/S Pos.: --
Date: 07/29/9"
17?
-------
e 1
3eak Area (A-s1: 4.3"""
Uank Corrected Pk Height (A): 0.184
Concentration (ug/L ): 4.7S4
Time: 12:44
Peak Height (A): 0.154
ig2
ID: 173-60-1B
Seq. No. : .00017
Dedicate 1
'eak Area (A-s): 0.059
Uank Corrected Pk Height (A): 0.002
;oncentration (ug/L ): 0.055
A/S Pos.: --
Date: 07/29/9"7
Time: 12:45
Peak Height (A): 0.002
ID: 173-60-1B D
Seq. No.: 00018
Replicate 1
3eak Area fA-s): 0.045
slank Corrected Pk Height (A): 0.002
:oncentration (ug/L ): 0.047
A/S Pos.: --
Time: 12:46
Peak Height (A): 0.002
Date: 07/29/97
ID: 173-60-18 MS
Seq. No.: 00019
leplicate 1
!eak Area (A-s): 4.567
lank Corrected Pk Height (A): 0.199
.oncentration (ug/L ): 5.183
A/S Pos.: —
Time: 12:47
Peak Height (A): 0.199
Date: 07/29/9"
ID: 173-60-18 MSD
Seq. No.: 00020
.eplicate 1
•eak Area (A-s): 4.636
lank Corrected Pk Height (A): 0.203
oncentration (ug/L ): 5.272
A/S Pos.: --
Time: 12:48
Peak Height (A): 0.203
Date: 07/29/97
ID: 174-97-oy jre *
Seq. No
eplicate 1
eak Area (A-s): 0.042
lank Corrected Pk Height (A):
oncentration (ug/L ): 0.039
0.002
00021
A/S Pos.
Time: 12:49
Peak Height (A) :. 0.00:
Date: 07/29/9'
g2
ID: 174-97-0/1=
Il.l-<.0-4ftl>
D Seq.
No
eplicate 1
eak Area (A-s): 0.029
lank Corrected Pk Height (A): 0.001
oncentration (ug/L ): 0.023
00022
A/S Pos.: --
Time: 12:50
Peak Height (A): 0.001
Date: 07/29/9'
ID: CCVl=6.0ug/L
Seq. No.: OO023
eplicate 1
eak Area (A-s): 5.399
lank Corrected Pk Height (A): 0.232
A/S Pos.: --
Time: 12:52
Peak Height (A): 0.232
Date: 07/29/9"
178
-------
sncantration (ug/L
0.041
g2
ID: CCB1
1
Seq. No
solicate
=ak Area (A-s): 0.009
lank Corrected Pk Height (A): 0.000
^ncentration (ug/L ): 0.005
00024
A/S Pos . : --
Time: 12:55
Peak Height (A): O.OOO
Date: 07/29/9^
32
ID: 173-60-4AB
Seq. No
=plicate 1
=ak Area (A-s): 0.009
lank Corrected Pk Height (A): 0.000
uncentration (ug/L ): 0.003
00025
A/S Pos
Time: 12:58
Peak Height (A): 0.000
Date: 07/29/9"
32
ID: 173-60-4AB D
Seq. No.: 00026
splicate 1
= ak Area (A-s): 0.010
Lank Corrected Pk Height (A): 0.000
sncentration (ug/L ): 0.000
A/S Pos.: --
Time: 12:59
Peak Height (A): 0.000
Date: 07/29/9
32
ID: 173-60-4C
Seq. No
Bolicate 1
=ak Area (A-s): 0.008
Lank Corrected Pk Height (A): 0.000
sncentration (ug/L ): 0.003
00027
A/S Pos.: —
Time: 13:21
Peak Height (A): 0.000
Date: 07/29/9
32
ID: 173-60-4C D
Seq. No
aplicate 1
;ak Area (A-s): 0.008
Lank Corrected Pk Height (A): 0.000
Dncentration (ug/L ): 0.008
00028
A/S Pos.: —
Time: 13:22
Peak Height (A): 0.000
Date: 07/29/9
32
ID: 173-60-4D
Seq. No.: OOO29 A/S Pos.: --
2plicate 1
;ak Area (A-s): 0.067
.ank Corrected Pk Height (A): 0.003
jncentration (ug/L ): 0.065
Time: 13:25
Peak Height (A): 0.003
Date: 07/29/9
ID: 173-60-4D D
Seq. No.: 00030
;plicate 1
:ak Area (A-s): 0.095
.ank Corrected Pk Height (A): 0.004
mcentration (ug/L ): 0.091
A/S Pos.: --
Time: 13:26
Peak Height (A): 0.004
Date. 07/29/97
179
-------
ID: 174 gy-
Sea. No.: 00031
A/S Pos . : --
Date: 07/29/9"
^eplicate 1
=eak Area (A-s): 0.020
Blank Corrected Pk Height (A): 0.001
Concentration (ug/L ):
0.023
Time: 13:27
Peak Height (A): 0.001
Hg
ID: 174-97-9/1
Seq. No.: 00032
Replicate 1
^eak Area (A-s): 0.015
Blank Corrected Pk Height (A): 0.001
Concentration (ug/L ): 0.013
A/S Pos.: --
Time: 13:28
Peak Height (A): 0.001
Date: 07/29/9
-\g2
ID: 173-60-2B
Seq. No.: 00033
Replicate 1
^eak Area (A-s): 0.070
Blank Corrected Pk Height (A): 0.003
Concentration (ug/L ): 0.070
A/S Pos
Time: 13:29
Peak Height (A): 0.003
Date: 07/29/97
Hg2
ID: 173-60-2B D
Seq. No.: 00034
Replicate 1
3eak Area (A-s): 0.078
Blank Corrected Pk Height (A): 0.003
Concentration (ug/L ): 0.081
A/S Pos.
Time: 13:30
Peak Height (A): 0.003
Date: 07/29/9
Hg2 ID: CCV2=6.0ug/L
Seq. No.: 00035
Replicate 1
aeak Area (A-s): 5.228
Blank Corrected Pk Height (A): 0.226
Concentration (ug/L ): 5.866
A/S Pos.: --
Time: 13:31
Peak Height (A): 0.226
Date: 07/29/97
Hg2
ID: CCB2
Seq. No
Replicate 1
3eak Area (A-s): 0.027
Uank Corrected Pk Height (A): 0.001
Concentration (ug/L ): 0.013
00036
A/S Pos.: --
Time: 13:32
Peak Height (A): 0.001
Date: 07/29/9"
ID: 173-60-28 MS
Seq. No.: 00037
Replicate 1
Jeak Area (A-s): 4.478
Slank Corrected Pk Height (A): 0.200
;oncentration (ug/L ): 5.186
A/S Pos.: --
Time: 13:34
Peak Height (A): 0 . 2OO
Date: 07/29/9
-------
>licate i
,K Area (A-s): 4.487
,nk Corrected Pk Height (A): 0.192
icentration (ug/L ): 4.982
Time: 13:35
Peak Height (A): 0.192
Seq. No
•licate 1
k Area (A-s ) : 0.036
,nk Corrected Pk Height (A): 0.002
centration (ug/L ): 0.039
00039
A/S Pos.: --
Time: 13:06
Peak Height (A): 0.002
Date: 07/29/9"
ID: 173-60-S&A- D
Seq. No.: 00040
!licate 1
k Area (A-s ) : 0.026
nk Corrected Pk Height (A): 0.001
centration (ug/L ): 0.029
A/S Pos.: --
Time: 13:38
Peak Height (A): 0.001
Date: 07/29/9'
ID: 173-60-5C
Seq. No.: 00041
licate 1
k Area (A-s): 0.024
nk Corrected Pk Height (A): 0.001
centration (ug/L ): 0.021
A/S Pos.: —
Time: 13:40
Peak Height (A): O.OO1
Date: 07/29/9'
ID: 173-60-5C D
licate 1
k Area (A-s): 0.027
nk Corrected Pk Height (A)
centration (ug/L ): 0.021
Seq. No.: 00042
0.001
A/S Pos.: --
Time: 13:41
Peak Height (A): 0.001
Date: 07/29/9"7
ID: 173-60-5D
Seq. No.: 0004;
licate 1
k Area (A-s) : 0.030
nk Corrected Pk Height (A): 0.001
centration (ug/L ): 0.029
A/S Pos.: --
Time: 13:42
Peak Height (A): 0.001
Date: 07/29/97
ID: 173-60-5D D
Seq. No.: 00044
licate 1
k Area (A-s) : 0.028
nk Corrected Pk Height (A): 0.001
centration (ug/L ): 0.023
A/S Pos.: --
Time: 13:43
Peak Height (A): O.001
Date: 07/29/9"
licate 1
k Area (A-s ) : 0.031
nk Corrected Pk Height (A): 0.001
Time: 13:44
Peak Height (A): 0.001
Date: 07/29/9:
ISi
-------
.oncentration (ug/L ): 0.023
io, \%j
ID: 174-97-10/2
Seq . No
'eplicate 1
Jeak Area (A-s): 0.025
:lank Corrected Pk Height (A): 0.001
oncentration (ug/L ): 0.02o
00046
A/S Pos.: --
Time: 15:45
Peak Height (A): 0.001
Date: 07/2° 9:
ID: CCV3-6.0ug/L
Seq. No.: 00047
;eplicate 1
'eak Area (A-s): 5.274
lank Corrected Pk Height (A): 0.229
oncentration (ug/L ): 5.939
A/S Pos.: —
Time: 13:46
Peak Height (A): 0.229
Date: 07/29/97
ID: CCB3
Seq. No.: 00048
eplicate 1
eak Area (A-s): 0.033
lank Corrected Pk Height (A): 0.001
oncentration (ug/L ): 0.023
A/S Pos.: —
Time: 13:47
Peak Height (A): 0.001
Date: 07/29/97
ID: 173-60-11AB
Seq. No.: 00049
eplicate 1
eak Area (A-s): 0.027
lank Corrected Pk Height (A): 0.001
oncentration (ug/L ): 0.029
A/S Pos.: —
Time: 13:49
Peak Height (A): 0.001
Date: 07/29/97
ID: 173-60-11AB D
Seq. No.: 00050
eplicate 1
eak Area (A-s): 0.026
lank Corrected Pk Height (A):
oncentration (ug/L ): 0.018
0.001
A/S Pos.
Time: 13:50
Peak Height (A): 0.001
Date: 07/29/9"
a2
ID: 173-60-11A
Seq. No.: OO051
eplicate 1
eak Area (A-s): 0.020
lank Corrected Pk Height (A): 0.001
oncentration (ug/L ): 0.013
A/S Pos.: —
Time: 13:51
Peak Height (A): 0.001
Date: 07/29/9:
ID:
173^-
60-llA D
Seq. No.: 00052
eolicate 1
3ak Area (A-s): 0.019
lank Corrected Pk Height (A): 0.001
oncentration (ug/L ): 0.013
A/S Pos.: --
Time: 13:52
Peak Height (A): 0.001
Date: 07/29/9:
182
-------
ID: 173-60-11D
Seq. No.: 0005:
A/S Pos.: --
Date: 07/29/9:
ilicate 1
.k Area (A-s ) : 0.045
ink Corrected Pk Height (A): 0.002
icentration (ug/L ): 0.047
Time: 13:53
Peak Height (A): 0.00:
ID: 173-60-11D D
Seq. No.: 00054
dicate 1
.k Area (A-s) : O.OS1
.nk Corrected Pk Height (A): 0.003
,centration (ug/L ): 0.07S
A/S Pos.: —
Time: 13:54
Peak Height (A): 0.003
Date: 07/29/9'
ID: 173-60-3B
Seq. No.: 00055
licate 1
k Area (A-s ) : 0.082
nk Corrected Pk Height (A): 0.004
centration (ug/L ): 0.091
A/S Pos.: --
Time: 13:55
Peak Height (A): 0.004
Date: 07/29/9'
ID: 173-60-36 D
Seq. No,
licate 1
k Area (A-s): 0.071
nk Corrected Pk Height (A): 0.002
centration (ug/L ): 0.063
00056
A/S Pos.: --
Time: 13:56
Peak Height (A): 0.002
Date: 07/29/97
ID: 173-60-36 MS
Seq. No.: 00057
licate 1
k Area (A-s): 4.491
nk Corrected Pk Height (A): 0.197
centration (ug/L ): 5.113
A/S Pos.: --
Time: 13:57
Peak Height (A): 0.197
Date: 07/29/9'
ID: 173-60-36 MS D
Seq. No.: 00058
A/S Pos'.
licate 1
k Area (A-s): 4.658
nk Corrected Pk Height (A): 0.210
centration (ug/L ): 5.454
Time: 13:58
Peak Height (A): 0.210
Date: 07/29/97
ID: CCV4=6.0ug/L
Seq. No.: 00059
A/S Pos.: —
Date: 07/29/97
licate 1
K Area (A-s): 5.259
nk Corrected Pk Height (A): 0.225
centration (ug/L ): 5.843
Time: 14:00
Peak Height (A): 0.225
ID: CC84
Seq. No.: 00060 A/S Pos.: --
Date: 07/29/97
183
-------
Dedicate
3eak Area
I
(A-s): 0 . 03o
31ank Corrected Pk Height (A): 0.001
3oncentration (ug/L ): 0.031
Time: 14:01
Peak Height (A): 0.001
HgZ
ID: 173-60-6A
C£
Seq . No
00061
A/S Pos.
Date: 07/29/97
3eolicate 1
3eak Area (A-s): 0.033
Blank Corrected Pk Height (A):
Concentration (ug/L ): 0.023
0.001
Time: 14:03
Peak Height (A): 0.001
Ha:
ID: 173-60-6A
t-VJ «*
Seq. No.: 00062
Dedicate 1
3eak Area (A-s): 0.035
31ank Corrected Pk Height (A): 0.001
Concentration (ug/L ): 0.029
A./S Pos. : --
Time: 14:04
Peak Height (A): 0.001
Date: 07/29/9'
ID: 173-60-6AC
Seq. No.: 00063
Replicate 1
3eak Area (A-s): 0.035
Blank Corrected Pk Height (A): 0.002
Concentration (ug/L ): 0.039
A/S Pos.: --
Time: 14:05
Peak Height (A): 0.002
Date: 07/29/97
ID: 173-60-6AC D
Seq. No.: 00064
^eolicate 1
3eak Area (A-s): 0.031
Uank Corrected Pk Height (A): 0.001
Concentration (ug/L ): 0.026
A/S Pos.: —
Time: 14:06
Peak Height (A): 0.001
Date: 07/29/97
ID: 173-60-6D
Seq. No
^eolicate 1
3eak Area fA-s): 0.149
;lank Corrected Pk Height (A): 0.006
:oncentration (ug/L ): 0.154
00065
A/S Pos.: —
Time: 14:07
Peak Height (A):' 0.006
Date: 07/29/97
ID: 173-60-6D D
Seq. No,
'.eolicate 1
'eak Area (A-s): 0.083
'lank Corrected Pk Height (A): 0.003
:oncentration (ug/L ): 0.081
00066
A/S Pos.: --
Time: 14:08
Peak Height (A): 0.003
Date: 07/29/97
ID: 173-60-7
Seq. No.: 00067
eolicate 1
eak Area (A-s): 0.051
lank Corrected Pk Height (A):
0.002
A/S Pos.: --
Time: 14:10
Peak Height (A): 0.002
Date: 07/29/97
184
-------
ncentration (ug/'L ): 0.047
ID: 173-60-7 D
Seq. No.: 00068
A/S Pos
Date: 07/29/9'
olicate 1
ak Area (A-s): 0.062
ank Corrected Pk Height (A): 0.002
ncentration (ug/L ): 0.060
Time: 14:11
Peak Height (A): 0.002
ID: 174-97-1/15
Seq. No
olicate 1
ak Area (A-s): 0.058
ank Corrected Pk Height (A): 0.003
"icentration (ug/L ): 0.073
00069
A/S Pos.: --
Time: 14:12
Peak Height (A): 0.003
Date: 07/29/9'
ID: 174-97-4/13 D
Seq. No.: 00070
olicate 1
ak Area (A-s): 0.061
ank Corrected Pk Height (A): 0.002
-icentration (ug/L ): 0.057
A/S Pos.: --
Time: 14:13
Peak Height (A): 0.002
Date: 07/29/9'
ID: CCV5-6.0ug/L
Seq. No.: 00071
Dlicate 1
ak Area (A-s): 5.275
ank Corrected Pk Height (A): 0.232
-icentration (ug/L ): 6.031
A/S Pos.: --
Time: 14:14
Peak Height (A): 0.232
Date: 07/29/9^
ID: CC85
Seq. No.: 00072
plicate 1
nk Area (A-s): 0.028
ank Corrected Pk Height (A): 0.001
icentration (ug/L ): 0.023
A/S Pos.: --
Time: 14:16
Peak Height (A): 0.001
Date: 07/29/9
ID: 42298 MB3
Seq. No.: 0007
slicate 1
Jk Area (A-s): 0.023
snk Corrected Pk Height (A): 0.001
icentration (ug/L ): 0.016
A/S Pos
Time: 14:20
Peak Height (A): 0.001
Date: 07/29/9
ID: 42298 MB3 D
Seq. No.: 00074
>licate 1
tk Area (A-s) : 0.014
ink Corrected Pk Height (A): 0.000
'icentration (ug/L ): 0.008
A/S Pos.: --
Time: 14:21
Peak Height (A): 0.000
Date: 07/29/9'
185
-------
ID: 42298 LCS3
Seq. No.: 0007!
A/S Pos.: --
Date: 07/29/9'
"Jeak Area (A-s): 4.57S
ilank Correctad Pk Height (A): 0.202
Concentration (ug/L ): 5.246
Time: 14:23
Peak Height (A): 0.202
Hg2
ID: 42298 LCS3 D
Seq. No.: 00076
Replicate 1
3eak Area (A-s): 4.458
Uank Corrected Pk Height (A): 0.190
;oncentration (ug/L .): 4.949
A/S Pos.: --
Time: 14:24
Peak Height (A): 0.190
Date: 07/29/9'
ID: 174-97-
•n cc
Seq. No.: 00077 A/S Pos,
Replicate 1
3eak Area (A-s): 0.069
slank Corrected Pk Height (A): 0.003
'.oncentration (ug/L ): 0.073
Time: 14:25
Peak Height (A): 0.003
Date: 07/29/9'
g2
ID: 174-97-£/4r5-^
Seq. No
^eplicate 1
•eak Area (A-s): 0.052
lank Corrected Pk Height (A): 0.002
.oncentration (ug/L ): 0.047
00078
A/S Pos.: —
Time: 14:26
Peak Height (A): 0.002
Date: 07/29/9'
g2
ID: 174-97-6/1
M
eplicate 1
eak Area (A-s): 4.385
lank Corrected Pk Height (A): 0.182
oncentration (ug/L ): 4.735
Seq. No.: 00079
A/S Pos.: —
Time: 14:27
Peak Height (A): 0.182
Date: 07/29/97
g2
ID: 174-97-6/1D l"lC
Seq. No
eplicate 1
eak Area (A-s): 4.513
lank Corrected Pk Height (A): 0.192
oncentration (ug/L ) : 4.988
OO080
A/S Pos:: —
Time: 14:28
Peak Height (A): 0.192
Date: 07/29/97
g2
ID: 174-97--t/4-i-
Seq. No.: 00081
eplicate 1
eak Area (A-s): 0.042
lank Corrected Pk Height (A): 0.002
oncentration (ug/L ): 0.039
A/S Pos.: --
Time: 14:31
Peak Height (A) : 0.002
Date: 07/29/9"
g2
ID: 174-97-1/11 P
Seq. No.: 00082 A/S Pos.: -- Date: 07/29/'=>'
-------
clicate 1
3K Area '. A-s ) : 0.040
ank Corrected P!~ Height (A): 0.001
ncsnt ration (ug/L ): 0.037
Time: 14:52
Peak Height (A): O.OO
ID: CCVl-o.Oug/L
1
Seq. No
olicata
aK Area (A-s): 3.325
ank Corrected Pk Height (A): 0.234
ncentration (ug/L ): 6.080
0008
A/
Pos . : --
Date: 07/29/9"
Time: 14:33
Peak Height (A): 0.234
ID: CCB1
Seq. No.: 00084
A/S Pos.: —
Date: 07/29/9
Dlicate 1
ak Area (A-s): 0.037
ank Corrected Pk Height (A): 0.001
ncentration (ug/L ): 0.031
Time: 14:34
Peak Height (A): 0.001
ID: 174-97-275-
Seq. No.: 00085
olicate 1
ak Area (A-s): 0.144
ank Corrected Pk Height (A): 0.006
-icentration (ug/L ): 0.146
A/S Pos.: --
Date: 07/29/9
Time: 14:35
Peak Height (A): 0.006
ID: 174-97-S
-
Seq. No
plicate 1
ak Area (A-s): 0.139
ank Corrected Pk Height (A): 0.006
-icentration (ug/L ): 0.149
00086
A/S Pos.: --
Date: 07/29/9"7
Time: 14:36
Peak Height (A): O.OOo
ID: 174-97-5/1^1
Seq. No.: 00087
Dlicate i
ik Area (A-s): 0.222
ank Corrected Pk Height (A): 0.009
-icentration (ug/L ): 0.227
A/S Pos.: --
Date: 07/29/9"
Time: 14:37
Peak Height (A)r O.OO9
ID: 174-97-SAL4— D
Seq. No.: 00088
plicate 1
IK Area (A-s): 0.221
ink Corrected Pk Height (A): 0.009
icentration (ug/L ): 0.242
A/S Pos.: --
Date: 07/29/9"
Time: 14:38
Peak Height (A): 0.009
ID: 174-97-iV-^
Seq. No.: 00089
>licate 1
;k Area (A-s): 0.254
ink Corrected Pk Height (A): 0.011
A/S Pos.
Date: 07/29/9"
Time: 14:43
Peak Height (A): 0.011
187
-------
Concentration tug/L ): 0.276
ID: 174-97-7/lu :
Seq. No.: O00°0
A/S Pos . : --
Date: 0^/29/9"
Replicate 1
3eak Area (A-s): 0.24"
Blank Corrected Pk Height (A): O.OiO
Concentration (ug/L ): 0.271
Time: 14:44
Peak Height (A): 0.010
ID: 173-60-4DE
Seq. No.: 00091
A/S Pos.: —
Date: 07/29/9'
Replicate 1
Deak Area (A-s): 0.021
Blank Corrected Pk Height (A): 0.001
Concentration (ug/L ): 0.013
Time: 14:45
Peak Height (A): 0.001
ID: 173-60-4DE D
Seq. No.: 00092
A/S Pos,
Date: 07/29/9:
Replicate 1
Deak Area (A-s): 0.024
Blank Corrected Pk Height (A): 0.000
Concentration (ug/L ): 0.010
Time: 14:46
Peak Height (A)
0.000
ig2 ID: 173-60-5DE Seq. No.:
Replicate 1
Deak Area (A-s): 0.033
ilank Corrected Pk Height (A): 0.001
Concentration (ug/L ): 0.037
00093
Time:
Peak
A/S Pos. : —
14:48
Height (A): 0.001
Date: 07/29/9~
<92
ID: 173-60-5DE D
Seq. No.: 00094
Replicate 1
'eak Area (A-s): 0.026
:lank Corrected Pk Height (A): 0.001
.oncentration (ug/L ): 0.029
A/S Pos.: --
Date: 07/29/9:
Time: 14:49
Peak Height (A): 0.001
g2 ID: CCV2=6.0ug/L
Seq. No.
'eplicate 1
'eak Area (A-s): 5.278
lank Corrected Pk Height (A): 0.233
oncentration (ug/L ): 6.046
00095
A/S Pos.: --
Date: 07/29/9"
Time: 14:50
Peak Height (A): 0.233
ID: CCB2
Seq. No.: OO096
eplicate 1
eak Area (A-s): 0.035
lank Corrected Pk Height (A): 0.001
oncentration (ug/L ): 0.034
A/S Pos.: --
Time: 14:51
Peak Height (A): 0.001
Date: 07/29/9"
188
-------
ID: 173-6C-6DE
Sec. No.: 00097
A/S Pos.: --
Date: 07, 29/o~
plicate 1
ak Area (A-s): 0.025
ank Corrected Pk Height (A): 0.001
ncentration (ug/L ): 0.018
Time: 14:52
Peak Height (A): 0.001
ID: 173-60-6DE D
Seq. No.: 00098
A/S Pos.
Date: 07/29/9~
olicate 1
ak Area (A-s): 0.029
ank Corrected Pk Height (A): 0.001
ncentration (ug/L ): 0.021
Time: 14:53
Peak Height (A): 0.001
ID: 173-60-6DE MS
Seq. No.: 00099
Dlicate 1
ak Area (A-s): 4.745
ank Corrected Pk Height (A): 0.205
•icentration (ug/L ): 5.316
A/S Pos.
Date: 07/29/9'
Time: 14:54
Peak Height (A): 0.205
ID: 173-60-6DE MSD
Seq. No.: 00100
plicate 1
ak Area (A-s): 4.649
ank Corrected Pk Height (A): 0.203
•icentration (ug/L ): 5.264
A/S Pos.: --
Time: 14:55
Peak Height (A): 0.203
Date: 07/29/c?"
ID: 173-60-11DE
Seq. No.: 00101
>licate 1
ik Area (A-s): 0.039
jnk Corrected Pk Height (A): 0.001
•icentration (ug/L ): 0.037
A/S Pos.: --
Time: 14:57
Peak Height (A): 0.001
Date: 07/29/9-
ID: 173-60-11DE D
Seq. No.: 00102
>licate 1
ik Area (A-s): 0.028
jnk Corrected Pk Height (A): 0.001
icentration (ug/L ): 0.016
A/S Pos. : —
Time: 14:58
Peak Height (A): 0.001
Date: 07/29/9^
ID: 173-60-6B
Seq. No.: 00103
A/S Pos.: --
Date: 07/29/9'
>licate 1
,k Area (A-s) : 0.026
;nk Corrected Pk Height (A): 0.001
centration (ug/L ): 0.021
Time: 14:59
Peak Height (A): 0.001
ID: 173-60-68 D
Seq. No.: 00104
A/S Pos.: --
Date: 07/29/Q-
189
-------
Replicate 1
Peak Area (A-s): 0.030
Blank Corrected Pk Height (A)
Concentration (ug/L ): 0.021
Time: 15:00
Peak Height (A): 0.001
0.001
Hg2 ID: CCV3-6 .Oug./L
Replicate 1
Peak Area (A-s'): 5.220
Blank Corrected Pk Height (A):
Concentration (ug/L ): 5.739
Seq. No.: 00105
A/S Pos.: --
Date: 07/29/9'
0.221
Time: 15:01
Peak Height (A): 0.221
Hg2
ID: CCB3
Seq. No.: 00106 A/S Pos.: —
Date: 07/29/9"
Replicate 1
Peak Area (A-s): 0.035
Blank Corrected Pk Height (A)
Concentration (ug/L ): 0.031
Time: 15:02
Peak Height (A): 0.001
0.001
190
-------
/Weight File: AB757.IDW
nple volume: 100 mL
_oc .
0
1
4
5
6
"7
3
o
10
11
12
13
14
15
16
17
IS
19
20
21
24
25
26
27
23
29
30
31
32
f /
•JO
34
35
36
37
38
39
Samole ID
STD 3LK
STDl=0.2ug/L
STD2=0.5ug/L
STD3=1.Oug/L
STD4=2.Oug/L
STD5=5.0ug/L
STDo=LO.Oug/L
ICV=4.Oug/L
ICB
CHECK LO
42293 MB4
42293 M84 D
4229S LCS
'42298 LCS D
173-oO-oA
1—* ~? ' ~" iL -* r\
/sj~"O
-------
Element File: HG_.nEL
'Element: Hg2
Print Data: Main+Suppl
0 rint; Ca1i b. Cu rve
Remarks:
STANDARDS^ 3-008-5
QC- 3-005-0
Anal/st: .-ICHAPDS
Peak Storage: None
H
INSTRUMENT: 5100
Wavelength: 233.7 Peak
Signal Type: -.-
Pead Time: 30.0
Sample Replicates: 1
Standard Replicates: 1
Technique: MHS
Slit: 0.7 Low
Signal Measurement:
Read Delay: 1.0
Version
'.01
Peak
Height ( 5 >
BCC Time: 2
-LAME:
Flame T/pe: Air
Oxidant Fl^ow: 10.0 L/min
Flame Sensor: On
Fuel Flow: 2.0 L/min
CALIBRATION:
Solutions ;
Calib. 8 lank
Standard 1
Standard 2
Standard. 3
Standard" 4
Standard 5
Standard 6
STD
STD
STD
STD
STD
STD
STD
Calibration Units:
Calibration Type:
ID
SLK
1
2
7*
4
c
6
Cone
0.200
0 . 500
1.000
2 . 000
5 . 000
10.000
ug./L Sample Units: ug/L
Linear
Matrix Check Calculations:
% Difference for Dupls: No Locations
'o Recovery for Spike: No Locations
Cone
192
-------
ment File: HG_.MEL Element: Hg2 Wavelength: 253."
.e: 07/31/97 Time: OS: 59 Slit: 0.7 L
a File: A6787.DAT ID/Wt File: AB787.IDW Lamp Current: 0
hnique: MHS Calib. Type: Linear Energy: 73
ark 1: STANDARDS- 3-008-5
iark 2: QC= 3-008-6
ID: STD BLK Seq. No. :; 00003 A/S Pos. : -- Date: 0//31/-7
licate 1 Time: 09:00
k Area (A-s): 0.000 Peak Height (A): 0.001
nk Corrected Pk Height (A): 0.001
centration (ug/L ): 0.016
o-;ero performed.
ID: STDl=0.2ug/L Seq. No.: 00004 A/S Pos.: -- Date: 07/31/9"
ple abs. is greater than that of the largest standard.
licate 1 Time: 09:01
k Area (A-s): 0.131 Peak Height (A): 0.007
nk Corrected Pk Height (A): 0.007
centration (ug/L .) : 0.223
ndard number 1 applied. [0.200J
relation coefficient: 1.00000 Slope: 0.0346
ID: STD2=0.5ug/L Seq. No.: 00005 A/S Pos.: — Date: 07/31/97
pie abs. is greater than that of the -largest standard.
licate 1 Time: 09:03
k Area (A-s): 0.452 Peak Height (A): 0.01S
nk Corrected Pk Height (A): 0.01S
centration (ug/L ): 0.528
ndard number 2 applied. [0.500]
relation coefficient: 0.99894 Slope: O.O363
ID: STD3=1.0ug/L Seq. No.: 00006 A/S Pos.: -- Date: 07/31/9"
ple abs. is greater than that of the largest standard.
licate 1 Time: 09:04
k Area (A-s): 0.911 Peak Height (A): 0.033
nk Corrected Pk Height (A): 0.038
centration (ug/L ): 1.046
ndard number 3 applied. [1.000]
relation coefficient: 0.99919 Slope: 0.0376
ID: STD4=2.0ug/L Seq. No.: 00007 A/S Pos,: -- Date: 07/31/97
ola abs. is greater than that of the largest standard.
licate 1 Time: 09:05
193
-------
Area (A-s ) : 1.837 . Peak Height (A> : 0.076
Blank Corrected Pk Height (A): 0.073
Concentration (ug/L ): 2.070
Standard number 4 applied. [2.-000]
Correlation coefficient: 0.9995o Slope: 0.038o
-\g2 ID: STD5 = 5 . Oug/'L Seq. No.: 00008 A/S Pos.: -- Date: 07/31/9"
Sample abs. is greater than that of the largest standard.
Replicate 1 Time: 09: Oo
seak Area (A-s): 4.675 Peak Height (A>: 0.195
Blank Corrected Pk Height (A): 0.195
Concentration (ug/L ): 5.065
Standard number 5 applied. [5.000]
;orrelatiqn coefficient: 0.99992 Slope: 0.0390
Ho 2 ID: STD6- lO.Oug/L Seq. No.: 00009 A/S PCS.: — Date: 07/'31/°7
Sample abs. is greater than that of the largest standard.
Replicate 1 Time: 09:08
Deak Area (A-s): 9.315 Peak Height (A): 0.395
Blank Corrected Pk Height (A): 0.395
:oncentration (ug/L ): 10.127
Standard number 6 applied. [10.000]
:orrelation coefficient: 0.99996 Slope: 0.0393
194
-------
;ment File: HG_.MEL Element: Hg2
;e: 07/51/97 Time: 09:08
:a File: AB787.DAT ID/Wt File: AB787.IDW
:hnique: MHS Calib. Type: Linear
iark 1: STANDARDS- 3-008-5
lark 2: QC= 3-003-6
Wavelength: 253.7
Slit: 0,7 L
Lamp Current: 0
Energy: 73
H Display Calibration - C: \flflJSER\flflJ ILES\ELEMENT\HG_,NEL
0.395-
0
n
«
8,
^
^^
,x'
\jf*\
— ""t-J rt J™
..-•"
X--
.0n, Linear
nr^' M Corn. Coef.: 8.99996
pE3^S3 Slope; 8,8393
B*r Concentration 18.888
4
1,
195
-------
lement File: HG_.MEL Element: Hg2 Wavelength: 253.7
ate: 07/31/97 Time: 09:10 Slit: 0.7 L
ata File: A67S7.DAT ID/Wt File: A8737.IOW Lamp Current: 0
jchnique: MHS Calib. Type: Linear Energy: 73
smark i: STANDARDS^ 3-008-5
;mark 2: QC= 3-008-6
:2 10: ICV = 4.0ug/L Seq. Mo.: 00010 A/S Pos. : -- Date: 07/31/97
iolicate 1 Time: 09:ii
sak Area (A-s): 3.614 Peak Height (A): 0.152
ank Corrected Pk Height (A): 0.152
^ncentration (ug/L ): 3.36b
•2 ID: ^ICB Seq. No.: 00011 A/S Pos.: — Date: 07/31/3"
•olicats 1 Time: 09:12
ak Area (A-s): 0.025 Peak Height (A): 0.001
ank Corrected Pk Height (A): 0.001
ncentration (ug/'L ,) : 0.023
2 ID.: CHECK Lu Seq. No.: 00012 A/S Pos.: -- Date: 07/31/9"
olicate 1 Time: 09:13
ak Area (A-s ) : 0.195 Peak Height (A): 0.007
ank Corrected Pk Height (A): 0.007
ncentration (ug/L ): 0.189
2 ID: 42298 M84 Seq. No.: OO013 A/S Pos.: — Date: 07/3l/9~
olicate 1 Time: 09:15
ak Area fA-s): 0.019 Peak Height ('A): 0.000
ank Corrected Pk Height (A): 0.000.
ncentration (ug/L ): 0.003
2 ID: 42298 MB4 D Seq. No.: 00014 A/S Pos.: -- Date: 07/31/9^
olicate 1 Time: 09:15
ai- Area (A-s): 0.016 Peak Height (A): -0.000
ank Corrected Pk Height (A): -0.000
-icencration (ug/L ): -0.003
I ID: 42298 LCS Seq. No.: 00015 A/S Pos.: — Date: 07/31/9"
clicate 1 Time: 09:17
ak Area (A-s): 4.322 Peak Height (A): 0.181
ank Corrected Pk Height (A): 0.181
ncentration (ug/L ): 4.592
ID: 42298 LCS D
Seq. No.: 00016 A/5 Pos.: -- Date: 07./31.''9'
196
-------
lies-e 1
k Area (A-s;: 4.555
nk Corrected Pk Height (A): 0.196
cent ration (ug/L ): 4.980
Time: 09:13
Peak Height (A): 0.19c
ID: 173-60-6A
Seq. No.: 00017 A/S Pos.: -- Date: 07/31/9"
k Area (A-s ! : 0.041
nk Corrected Pk Height : 0.022
k Corrected Pk Height (A): 0.001
A/S Pos.: --
Time: 12:52
Peak Height (A): 0.001
Date: 07/31/9'
197
-------
-------
-------
-------
Appendix D
Gravimetric Analysis Data
cah/KA7997\03\07-RPT\APX-CVR WP6
-------
-------
/TV
Filter
TareWt
Number
6/18/97
TareWt
6/19/97
Difference
001
002
003
004
005
006
-£LS
007
008
-Ov
-G-
009
010
011
012
013
014
015
016
-Cub
017
018
019_
020
021
022
023
024
025
.a
-------
Project No..
Book No..
TITLE
om Page No—
Of.
!, 170/3
V^L-OL
0,
o3
Sample ID
LTV-01
LTV-07
LTV-13
LTV-19
LTV-25
LTV-31
LTV-37
LTV-44
LTV-50
LTV-83
LTV-100
Beaker #
2
3
4
5
6
7
8
9
10
11
12
Weigh 1
7/13/97
178.8614
171.5307
168.3872
152.5475
166.7439
180.5858
150.2989
167.4812
159.2096
148.3343
183.4912
Weigh 2
7/14/97
178.8619
171.531
168.3869
152.5471
166.7443
180.5861
150.2988
167.4815
159.2097
148.3345
183.4914
Difference
-0.0005
-0.0003
0.0003
0.0004
-0.0004
-0.0003
0.0001
-0.0003
-0.0001
-0.0002
-0.0002
beaker
1
2
3
4
5
6
7
8
9
10
11
12
weigh 1
7/10 Sam
174.9331
178.8372
171.5022
168.334
152.2608
166.2397
180.0437
150.2905
167.4813
159.2087
148.3343
183.4436
weigh 2
7/10 1pm
174.9327
178.8369
171.5022
168.3342
152.2605
166.2399
180.0439
150.2906
167.4809
159.2089
148.3341
183.4436
Difference
0.0004
0.0003
0
-0.0002
0.0003
-0.0002
-0.0002
-0.0001
0.0004
-0.0002
0.0002
0
To Page No.
lessed ft Understood by me.
Date
-------
Appendix E
Field Data
E.1 Method 23 and Method 29 Field Data Sheets
E.2 Meter Box Calibrations
E.3 Chain-of-Custody Sheets
E.4 Summary of Sampling Parameters
cah/K:\7997\03\07-RPTWX-CVR.WP6
-------
Appendix E.1
Method 23 and Method 29 Field Data Sheets
cah/K \7997\03\07-RPT\APX-CVR WPS
-------
/^SCI\W
/ "E«« *«e,rch Group. ,nc MODIFIED METHOD 5 DATA SHEET
Plant
Date
Operator
Sampling Location
Sample Type
Run Number
Static Pressure (±) (in. H2O)
Barometric Pressure (in. H2O)
l& L.T(/
(.'•L^-r?
rt/t- „
^JTi-f <
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Traverse
Point
Number
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3
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7?
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Time
(min)
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Time
(24hj)
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t?.t*
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f-tifji?
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tirfi
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Differ
(delta H,
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/ ^f-
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/, f 'f
ij?1*
£& i t£
'
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in.H20)
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f" ? S
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Temp.
(•F)
*t. ?^
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7 '•* j
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1 {.fl
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2-5'^
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X"' <^ .
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Trap
Temp.
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f^S)
/ C/'
C, X
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4 4?
^ £.
' k
fFf^
— — —
i.-^
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7*^
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Run
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Diagram of Duct
5 Meter
Outlet
(Tmout)
f"'~
/*T C^
•? <^.
fc'SJ
'£'(/
PL/
9 T'^"
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40 Nqents:
^ \
-------
Eastern Research Group. Inc
MODIFIED METHOD 5 DATASHEET
Run
Plant
Date
Operator
Sampling Location
Sample Type
Run Number
State Pressure (±) (in. H2O)
Barometric Pressure (in. H2O)
ST~-'/
-7 f 1- <-:»xl
M^V "
5 a-c..^
tinVi/J
XAD Trap Number
Filter Heater Setting (°F)
Probe Length & Type
Probe Heater Setting (°F)
Minimum Sample Volume (ft3)
Initial Leak Check
Final Leak Check
I Meter Box Number
Meter delta H @
DGM Factor (Y)
Nozzle Type & ID (in.)
Ambient Temperature (*F)
Assumed Moisture (% H2O)
K-Factor
// fo
Diagram of Duct
Schematic of Traverse Point Layout
Read and record all data every ' C> minutes
Traverse
Point
Number
ft f
,
Z-'
Is
-!,
T
K r
Sampling
Time
(min)
c;
,-o
If
-1,0
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7nS>
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Clock
Time
(24hr)
f(*0!
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tfy*'i
(Lar
>£'
UOI . $ "Is
£»f>&> *)?
q/&. f <>
y-7^ &OO
/•"///^ ./
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Head
((delta Ps),
in.H2O)
. Lr<-<
.> ^y
„ & 1
S^U
; f5
f " °>
t i
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-
Stack
Ts
(•F)
//T
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in
((7
/I*"-"
111
#*O r
.
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Differ
(delta H,
Desired
/. £/
/, -i-/
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f <-L
/. K[ •>
/0'=)
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£ a^f ,
'ressure
ential
in.H2O)
Actual
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Temp.
CF)
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Temp.
(°F)
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(of.
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6?g
DryGa
Inlet
(Tm in)
^ ^ '-.'
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Oirdet
(Tmout)
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Impinger
Exit
Temp.
CF)
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C*K
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Pump
Vacuum
(in.Hg)
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C,X
7- &
7,o
7./o
-------
Eostom Research Group- *«.'
MOISTURE RECOVERY FORM FOR METHOD 4
Plata
Uale
Sampling Location
Sample Ttffc
Implner Box Number
Recovery Rinses
Sample WentiflcatJon
Filter Number
XAD Number
Ovx-VVe-V
3*
LTV/
3 "4-10
60)0.4
t
Mq^.3>
"iM^.o
Total Weight Gain (g)
Weight
Gain
>(g)
330.1
-M-0»
^.\
^•°\
56.. 3
3»«-«
-------
Eastern Research Group, Inc.
MODIFIED METHOD 5 DATA SHEET
Run
Page 1 of
Plant
Date
Operator
Sampling Location
Sample Type
Run Number
Static Pressure (±Kin. H2O)
Barometric Pressure (in. H2O)
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/> •"
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Point
Number
K i
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t-
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Time
(min)
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to
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bfl
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Time
(24hr)
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Filter Heater Setting (°F)
Probe Length & Type
Probe Heater Setting {°F)
Minimum Sample Volume (ft3)
Initial Leak Check /? . /)£?,.
Final Leak Check /? ff)/f /
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Meter Box Number
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DGM Factor (Y)_
Nozzle Type & ID (in.)
Ambient Temperature (°F)
Assumed Moisture (% H2O)
K-Factor
i
Schematic of Traverse Point Layout
Read and record a!! data every ff> minutes
Velocity
Head
((delta Ps),
in.H2O)
* / O
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,75
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Differ
(delta H,
Desired
/,*-
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/,lf-^^-
•/,??
f.Z~>
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(°F)
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Trap
Temp.
(°F)
^ ^
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Diagram of Duct
s Meter
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Comments:
-------
Eastern Research Group. Inc
MODIFIED METHOD 5 DATA SHEET
Run
Page 1 of
Plant
Date
Operator
Sampling Location
Sample Type
Run Number
Static Pressure (±) (in. H2O)
Barometric Pressure (in. H2O)
Oiortis
-t.
XAD Trap Number
Filter Heater Settingi'F)
Probe Length & Type
Probe Heater Setting (*F)
Minimum Sample Volume (ft3)
Initial Leak Check
Final Leak Check
Meter Box Number
Meter delta H @
DGM Factor (Y)
Nozzle Type & IDJin.)
Ambient Temperature (QF)
Assumed Moisture (% H2O)
K-Factor
L'-r:
/, *£>
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/
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in.H2O)
^n^
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Ts
(°F)
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in.H2O)
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Temp.
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-------
Eortwn R^nach Group.
1 MOISTURE RECOVERY FORM FOR METHOD 4
Plant
L-TV
Samp ing Location
Samp
RunNurnM
Implnger Box Number
DoJn
Recovery RJnst
Sample IdenUflcatlon
LTV-
" , " ,
Impinger
Number
1
2
3
4
5
6
7
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MT
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Configuration
"- -.^
-------
^Eastern Research Group. In, MODIFIED METHOD 5 DATA SHEET
Plant
Date
Operator
Sampling Location
Sample Type
Run Number
Static Pressure (±) (in. H2O)
Barometric Pressure (in. H2O)
f*p» / //
£' (.'./"• *? /"
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(24hr)
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Filter Heater Setting (°F)
Probe Length & Type
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Minimum Sample Volume (ft3)
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Final Leak Check &•()/
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Diagram of Duct
Schematic of Traverse Point Layout
Read and record all data everv / ?~> minutes
Velocity
Head
((delta Ps),
in.H20)
„ '75
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• 1 '7
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t,7-"
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in.H2O)
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Temp.
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Comments:
-------
Eastern Research Group. Inc. —
MODIFIED METHOD 5 DATA SHEET
Plant
Date
Operator
Sampling Location
Sample Type
Run Number
Static Pressure (±)iin. H2O)^
Barometric Pressure (in. H2O)
&fZS .
X-^V? '
'*.£&
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Time
(24hr)
tlrVk.
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Meter
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r'/?A ^7%
7/ % r7 %
~77.r> - O£\
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-7 ^^^f^
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Head
((delta Ps),
in.H20)
- "T.^
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t Kfo
i ft'SL^'
-
Stack
Ts
CF)
/ /^
/7/
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7/Z
y/ ^
.
Orifice F
Differ
(delta H,
Desired
/.C/t-
/* £5
f C1^
/ "^r'L-
(,*,£-,
/• A/^.
'ressure
ential
in.H2O)
Actual
/fy-^
f.Ll
/ ^ ~is
f/<''^
ft 'er
^r
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<~ f-J
J rt
-------
&ERG
Eastern Research Group. Inc.
MOISTURE RECOVERY FORM FOR METHOD 4
Plant
Pate
Sampling Location
Sample Type
Recovery Plrionf ;,>
Samle Identification
Filter Number
XAD Number
L A'v
V . fc x>
0 ii tf>
Impinger
Number
1
2
3
4
5
6
7
Impinger
Solution
**
\\zO
^
MT
S«T
Amount of
Solution
}(g)
—
- ,n
- ,UO.^
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Impinger Tip
Configuration
K.O
^
GS
GS
OS
ImpinflerWerc
Final!
(g) ••»•
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t^ /*: (^ \
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SM
t 1 ^o v^ ^J
ifj *» ^^
initial ;
^l^
551.3
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M,,S
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Total Weight Gain (g)
hi-r^S"
Weight
; G?ln
IIC-S
O. &
-fc. 1
,-?
MY.<
3,,.,
-------
Eutem Research Croup. Inc.
MODIFIED METHOD 5 DATA SHEET
Run
Page 1 of
Plant
Date
Operator
Sampling Location
Samole Type
Run Number
Static Pressure (±) (in. H20) ^
Barometnc Pressure (in. H2O)
/T/y
t-7-<- ?''
t'J < v
O ,
Final Leak Check tf. Off '
t*£^ f~*
?*•»£&
1'^ 5
'/*tT
verses
Meter Box Number
Meter delta H @
DGM Factor (Y)_
Nozzle Type & ID (in.)
Ambient Temperature (*F) ;,
[Assumed Moisture (% H2O)
K-Factor
/~- .-<•
/
,c ^
?-/^_5
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..^\vjT:
V
3&t- ' 5 £. / Diagram of Duct
Read and record all data every / £>m , minutes
Traverse
Point
Number
£> •£
»,
L,
L~
t
1
Jff
'jl -7
-t.
„
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— f^y~
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/
4
Sampling
Time
(min)
£)
' Q
t- O
3£>
¥ O
/ c/
Co
SJ
!£>
~ iy
(/o
c £>
/- ^
— o
ID
iJ i>
^ C'
(yl^
Clock
Time
(24hr)
fr&Z. ()
fl^ U A,
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/ {? *3 S)
lo ;d
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, -7 -f A
'- •*" ~ £
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/ Z. 5^ti>
/'•^C'i"i
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Meter
Reading
((Vm),ft3)
't 7 ^ , 7. ^ -^
^-^^ "^6^
/^T -i/J,
•f.7/'. S/-
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/ ''•>/•
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Velocity
Head
((delta Ps),
in.H2O)
^.tj i-
P "
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j?/^ »
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A T „
/. "?
-
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7 / *?
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// '7
Orifice F
Differ
(delta H,
Desired
/ T T
/ 7--^
/• ^ /
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y-X^ «
/. Z-"7
/. 7 71
A 5 /
/.ff>
/ /P
^ f)1^
^r^~7~~
7 ^ ^
/ < ^
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ential
in.H2O)
Actual
/'/- T
/ T
/> ^7
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A ^J,
,,
' '/ ' jr^r
/. /^- /_
/ 7-- '
/• i- /
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/ ' ^"
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/ £x/
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Temp.
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77 <'
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r.r:^
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'£">(./
L-~? k>
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7, -O
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Temp.
CF)
L^^J
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'f^ ^
7-£->f>
7 5~^
7-5 f-S
£6, ^
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7*1 o
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Trap
Temp.
X//7
^^
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/ ^<^- <•
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1
1
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Inlet
(Tm in)
ft~7s
f3£
"^y
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JZ'Z,
£>,~7
(£?.'
Pump
Vacuum
(in.Hg)
•&,/}
> ' &
5' £>
~> ' CJ
?'*
f ' i-N
7 -/-
r ^
•^r
•f,
-------
EoJtem RasBorch <3»oup. Inc.
MOISTURE RECOVERY FORM FOR METHOD 4
Date*
Sampling Location
Sample Type .
Implngef Box Number
Sample Identmtatlon
Filter Nurriber;
X&ftKuiribtf
Li
Wk»
L I v -
m
"SiUr^
tei
Amount 6f
Solution
,;:.,;.igi:.-:;
~
~»-AOO\^
5CU-M
5-B5.3
i
^ I . Z.
5
-------
Eastern Research Group. Inc
MODIRED METHOD 5 DATASHEET
Run
Page 1 of
Plant
Date
Operator
Sampling Location •
Sample Type
Run Number
I Static Pressure (±) (in. H20)
I Barometric Pressure (in. H2O)
/Jl'
*~r^
{ti&faj*
XAD Trap Number
Filter Heater Setting (°F)
Probe Length & Type
Probe Heater Setting (°F)
Minimum Sample Volume (ft3)
/•z, I Initial Leak Check
Final Leak Check
Meter Box Number
Meter delta H @
DGM Factor (Y)
Nozzle Type & ID (in.)
Ambient Temperature (°F)
Assumed Moisture (% H2O)
K-Factor
f$*>*r
f^^
Gas
Meter
Reading
((Vm).ft3)
WS2
t.tb,P''f.1
/st.z*
T5f«f "2-
fVf.L (_
is?*i2<
7^-f,?"
i I !
Velocity
Head
((delta Ps),
in.H20)
t (3 /
.> 6. >
<&?
- &%
*• / 5
, -TS-
-
i
Stack
Ts
CF)
///
A^T
tfj
//^
//'/
//•?
-
Orifice F
Differ
(delta H,
Desired
— 1-..+.,,^
'' T^
// ± ->
I'St
f,75
?,S?>
', <"*>
'ressure
ential
in.H2O)
Actual
/,^//
/,?•>
/.^
/JJT^
/.^
Probe
Temp.
CF)
f,?c
i,^^
Z,«
?ZT^
^7-
^
L~£/£>
^&
Adsorbent
Trap
Temp.
CF) ,
DryGa
Inlet
(Tmin)
ftf
(&C/
/0£
'0$
f&7
tf>fl
$ Meter
Outlet
(Tmout)
?§
^^
"fOK
f/J^>
7nt
&7^
Impinger
Exit
Temp.
CF)
/•~"?
/-//
^>(^
^^7
%"7
(orj
Pump
Vacuum
(in.Hg)
?.<:>
f,&
\*
?f*
r(&
*.£
Comments:
-------
Eastern Research Group. Inc.
MODIFIED METHOD 5 DATA SHEET
Run
Page 1 of
I Plant
[Date
| Operator
[Sampling Location
! Sample Type
IRun Number
I Static Pressure (±) (in. H2O)
i Barometric Pressure (in. H2O)
.:.,.< " |XAD Trap Number ££&.
u.-t. '-' / | Filter Heater Setting (°F)
.'*' t& I Probe Lenath & Type
'"^3£. I Probe Heater Setting J"F)
/^fj/5/5 | Minimum Sample Volume (ft3)
"5 I Initial Leak Check f> C£>
tS? ,?>S\
^•' t> ,
7, 4/c-Sl
-v/r 7~f5
7 c-/V^'
Meter Box Number
Meter delta H @
DGM Factor (Y)
Nozzle Type & ID (in.)
Ambient Temperature (°F)
Assumed Moisture (% H2O)
J. , • •*&> | Final Leak Check fr^iti V ef" ^'iK-Factor
/'^
'/. 5r-£
, 'rfff
. ^ 7
^^
st>~?<:>
•J. 0$
P
«K
CT r
"-V
£ f , 4'.'? | *DiasramofDuct
Schematic of Traverse Point Layout
Comments
-------
Eastern Research Group. Inc.
MOISTURE RECOVERY FORM FOR METHOD 4
M 1 M k~h & "* " *%% <• •>
w* 1 A tt i "" ** ** •* y •*"* <^s "**' *''"'* ' **
? f**M«( > -^ -s-W...-. ^"vsa-i^u < ^ *•
riafo M f ^^t^^tt^* '
Sampling Location
Sample Type ;K „
Run Number «, ;—.;;; ,
Impinger Box Number
Recovery Partbit ,*,...> ,
Recovery Rinses ;
Sample Identification
Filter Number , ;/
XADNumbec ,
U\\J 6Vc-c-l
U\7.t»»«H-q
iOix4l<»»-
T3-I.1
y
Initial
(g)
U^.o
5"ig>.8
•5TS.S
i
M(^3L3,
60^.3
5^5.0,
p6,3.>
Total Weight Gain (g)
ht «'"„
Weight
Gain
(g)» .,-
J3Z -i
IVJ 3
^3V
?• /
Z.4
D.I
•ZV-Z-
3
-------
Eastern Research Group. Inc.
MODIFIED METHOD 5 DATASHEET
|Run
| Page 1 of
Plant
Date
Operator
Sampling Location
Sample Type
Run Number
Static Pressure (±) (in. H20)
Barometric Pressure (in. H2O)
Lfrr
fr-U-t'/
Wfcj/'
X'<^J~
*
XAD TrajJ Number
Filter Heater Setting (°F)
Probe Length & Type
Probe Heater Setting (°F)
Minimum Sample Volume (ft3)
Initial Leak Check
Final Leak Check
Meter Box Number
Meter delta H @
DGM Factor (Y)
Nozzle Type & ID (in.)
Ambient Temperature (*F)
Assumed Moisture (% H2O)
K-Factor
Z.n5
Diagram of Duct
Schematic of Traverse Point Layout
Traverse
Point
Number
/> «,
2,
*-t
*•
1
.
Sampling
Time
(min)
• ft
&
•^n
v-n
L/>
Clock
Time
(24hr)
/<*!, 5
fU.ufr
*$&.
(£f\b
f'< /£
ft ^5
(*> 15
Gas
Meter
Reading
((Vm),ft3)
&%?.•?'?'
<£ 9 7. 5
^7/ ,??
T"? ^ &$
<---o*- p "7
^»/ , yy;
5r^?y<
6,0t
Velocity
Head
((delta Ps),
in.H20)
tfc*
L;l^
**> <
,^a
* c= H
if-, !•$
*i oJ-
-
Stack
Ts
CF)
i/#
>//
//?
777
/"/'/'
ff C-,
1»
Orifice P
Diffen
(delta H,
Desired
— / " •+ —
(' L-0>
/, •?. ^
y,<*
/, ^^
f ^ /
•r^;^
7^-
-^^?r
•TJ,^
Adsorbent
Trap
Temp.
^
/
1
r
i
!
!
1
1
/
•
i
Dry Gas
Inlet
(Tm in)
3?
f *
^"9
/Y?7.
'/rf
///?
Meter
Outlet
(Tmout)
#-7
c O
rS
(Q«\f
(sy
5>CJ
T-<^
v^
"./%
Comments:
-------
Eastern Research Group. Inc.
MODIFIED METHOD 5 DATA SHEET
Run
Page 1 of
Plant
Date
Operator
Sampling Location
Sample Type
Run Number
Static Pressure (±) (in. H2O)
Barometric Pressure (in. H2O1
L '-"
£'£•/->-/ /
SI* t *
i'r pck
tf'S-Tl '?
"
- /£ 5
-'•^ ^5
XAD Trap Number
Filter Heater Setting (°F)
Probe Length & Type
Probe Heater SettngJ'F)^
Minimum Sample Volume (ft3)
Initial Leak Check
Final Leak Check
///£
< .'/, "r~
^_' « Af /
^^ rij
i/, Ollrf'
0 ./)/) ~f
Meter Box Number
Meter delta H @
DGM Factor (Y)
Nozzle Type & ID (in.)
Ambient Temperature (°F)
Assumed Moisture (% H2O)
K-Factor
£<-~g
/< * '-*
j -+
'<-/ /
s/
//' If
£ ., ^75^
•O^
^? 7" ^ Diagram of Duct
Schematic of Traverse Point Layout
Read and record all data every ^ minutes
Comments:
-------
feERS
Eastern Research Group. Inc
MODIFIED METHOD 5 DATA SHEET
Run
Page-lof
Plant
Date
Operator
Sampling Location
Sample Type
Run Number
Static Pressure (±) (in. H20)
Barometric Pressure (in. H2O)
<_-rv
L- ^5-^-1
Mte ',
~v /-c<--
rUtt/S
1
•
XAD Trao Number
Filter Heater Setting (°F)
Probe Length & Type
Probe Heater Setting (°F)
Minimum Sample Volume (ft3)
Initial Leak Check
Final Leak Check
Meter Box Number
Meter delta H @
DGM Factor (Y)
Nozzle Type & ID (in.)
Ambient Temperature (°F)
Assumed Moisture (% H2O)
K-Factor
l-sO?
Diagram of Duct
Schematic of Traverse Point Layout
Read and record all data every ./f minutes
Traverse
Point
Number
(L> ~>
•*?
foO
*^
!'•
!(,<(? -
n o&
&
Gas
Meter
Reading
«Vm).tt3)
Sf/,// ^
V(& .(it
<-so ,* 5&
<#G,7.1
u.?^// <
\S^J
Velocity
Head
((delta Ps).
in.H20)
,65
/. L^
', ^ b
. 7-r>
/ W
L- (Ty
/?
. ^ ,
'-*/.'
-
Stack
Ts
CF)
f't-o
ft"
//"/
VZV
110
ttO
J'J -" &
-'- -(.f
.
Orifice P
Differ
(delta H,
Desired
/,--
AZ7
/^
/ u^>
y.-s'-':
*t~t<
/
v— 0
1 •' /
;/ ,,^://
ressure
ential
in.H2O)
Actual
ft*-?
/.•;•?
/. ^3
/. ^'>
V/-H7
^7*
"?
''•fa*
.i-is===
Probe
Temp.
CF)
Z,Z.C
-Z^l^
't.L^
"LZ-S
'U^y
L<°'5
-»-^ -f~>
*s*?4z
Fitter
Temp.
CF)
17^
76,^
f^?^
7 ~~+
"iJ*t,
TJ,'^-
& //,J &f
Adsorbent
Trap
Temp.
(*F)
•
o Us*. L
i/
Dry Gas
Inlet
(Tmin)
?5
/r>v
//•&
//-
(rt
/s-7
O^>
'J
\ Meter
Outlet
(Tmout)
^T
tfl
(£>^
/f)£
/rtZ.
/A-?
/
V ' /
^bS>S
Impinger
Exit
Temp.
CF)
5~7
f~>
6>'L-
&~7
f*0
6~e
&
s
Pump ',
Vacuum !
(in.Hg) j
T//^
5,^>
5/.5^
?", 5
^.^
7.'-»"
\
-------
Eojfam Research Group. Inc.
MOISTURE RECOVERY FORM FOR METHOD 4
^j[ *s(nr
flam
ux.
diauv^
Sampling Location
Sample Type
Run
ImplngerBoxNumbef
Recovery Rinses
"3 * u-1 o
Sample IderttificaUon
LTV-
Filter Number
XAD Number,
QO*
AJA
Impinger
Number
1
2
3
4
5
6
7
Jmpinger
Solution
MT
5^ t\*oc>3
) DYo UzO2
5%. hMo1^
ICft \-\iOa
MT
M% KUKOH
IO%H^OS
MV« TNKJLnOq
^% \AiSoH
^lliccx
6e|
Amount of
Solution
(g)
~ N^Oc.
A
~teoa
—
-»oo^
-^
-Z50n
Impinger Tip
Configuration
Ko
<^Ak5
G5
Gs
NA&5
&s
GS
Impihger Weight l:^;;, *
Final
(g)
SC12.5
"7SM-0
697.6
M^T-.Z
5(pM
UO^.T_
^.^-H
Initial
f. ,(g)
MUI-M
^cn.i
5'n.^
i
MB^.B
5uuco
(jO(0-<9
l^lM.^-
Total Weight Gain (g)
Weight
ditrt
«g)
\>o.R
It^-S
iq- 1
(0.4
I.?
?.7.
34- >
'/•'M
-------
Eastern Research Group. Inc.
MODIFIED METHOD 5 DATA SHEET
Kun
Page " of
Plant jCTV-CrucisjrC |XAD Trap Number
Date
Operator
Sampling Location
Samole Type
Run Number
Static Pressure (±) (in. H2O)
Barometric Pressure (in. H2O)
fe/ZS/Cj >-
K\\»JV<
(NwtLT
01 (Y\4£taL&,
3± (
* — ">• (o"
MA / 2.0,. 3. fe
Filter Heater Setting (°F)
Probe Length & Type
Probe Heater Setting (°F)
Minimum Sample Volume (ft3)
Initial Leak Check
Final Leak Check
— — [Meter Box Number
2.SO
S'PrKc*
Z$o
M/A
,C/?<@iC'
•cOj^.s"
Meter delta H @
DGM Factor (Y)
Nozzle Type & ID (in.)
Ambient Temperature (°F)
Assumed Moisture (% H2O)
K-Factor
A. —o
f ."VI '
,«\SM
. ( oJ
90°
4,7-
c*cSrfe
fee" y r
/-»<. ^^^
re"
^i
|^.
1 C-O T. * l.£ Qi,~ /°. ('"""fbvwT Diagram of Duct
Schematic of Traverse Point Layout
Read and record all data every minutes
CD-.. ~
r '*f
Traverse
Point
Number
Sampling
Time
(min)
Clock
Time
(24hr)
Gas
Meter
Reading
((Vm),ft3)
. i Z
Veloctty
Head
{(delta Ps),
in.H2O)
Stack
Ts
CF)
Orifice Pressure
Differential
(delta H. in.H2O)
Desired
Actual
Probe
Temp.
Filter
Temp.
Adsorbent
Trap
Temp.
("F)
Dry Gas Meter
Inlet
(Tmin)
Outlet
(Tm out)
Impinger
Exit
Temp.
(•F)
Pump
Vacuum
(in.Hg)
A- i
f.O
2.-.S
S3
•7J
1 "
: S
30
1 C ' 0 \
3r*f
•7^-g
,3d
S 's
yo
y. I,")
.10 ft
**
/ o : sw
L^/v
'i'./O
i £ , 0
xyo
•Oj
O
no
t3'.oc
•=?, 3T
m.
JJ=0_
~yr
-23-
\%c
"rVTF
TTT
13.
^
P, :
5S!
2
,-/g i
S
Jii
flfr
U'
xi
io
c.
*
L?;gpi ?/
E
5
&!'»
Comments:
-------
Eojtem Reswoch Group. Vic.
MOISTURE RECOVERY FORM FOR METHOD 4
Plant i
Date. .<,-;,. ;. „ -,
Sampling Location
Sample Type
l$un Number ,,', %
Implnger Box Number
ftecovefy^ersdtt ; \
Recovery Rinses
Sample Identification
Filter Number :.
XAD Number
L~\ V Ske-l
Lt(&&\<*t-^
\nVei-
(Uefc.a.5
1
Irvle*
J 5 co . (- v-
^> * O.lkJ J-\^oU-i
LTV -
oo^-
K3A
Impinger
Nuhnbist
Impinger
Solution
Amount of
Sdlutibrt
(gj
Impinger Tip
Configuration
Impinger Weight
Final
Initial
Weight
Gain
(g)
100.
-------
i^^..- Eastern Research Group. Inc
MODIFIED METHOD 5 DATASHEET,
Run
Page 1 of
Date
Operator
Sampling Location
Sample Type
RUn Number
Static Pressure (±) (in. H2O)
XAD Trap Number
_L^
Filter Heater Setting^'F)
Probe Length & Type
Probe Heater Setting (*F)
MiRimum Sample Volume (ft3)
Initial Leak Check
Final Leak Check
'Meter Box Number
0,01610
Mfeei delta H@
Factor (Y) '
Nozzle Type & ID (in.)
Ambient Temperature (*F)
Assumed Moisture (% H2O)
K-Factor
>tQ3
%:£ Barometric Pressure (in. H2O)
Schematic of Traverse Polqt Layo
Read and record all data every |i f^-n minutes
=->.0
)
" Diagram of Duct
r.S,3.(
Traverse
Point
Number
Sampling
Time
(min)
Clock
Time
(24hr[
Gas - .
Meter
Reading
«Vm),tt3)
- Velocity
Head
((delta Ps),
in.H2O)
Stack
Ts
CF)
Orifice Pressure
Differential -•—-'•
' (delta H, in.H2O)
Desired Actual ^
Probe
Temp.
CF)
Filter
- Temp.
C'F) _
Adsorbent
Trap "j
Temp/
~._D$ Gas Meter ^
'" Inletlp%&""'"
(Trnln)~
:(Tmout} -
Impinger
' Bat -
,-Jemp...
-> rn -.
. Pump
Vacuum
(in.Hg)
4-
3-0
4A5
z^,^
_i£j
3E
4^
JZ
77
1M£
-i^
3
/.A
Jan
^/.
44
2
4LJ
Ji
^^_
LW
tt
%
2
IV.
1
XJt
Comments:
-------
Eastern Research Group, Inc. •
MOISTURE RECOVERY FORM FOR METHOD 4
PlStfU %> ,>'"lV4-,"4 ^ "^ ^
fiat A ' ' "3 '*jf»
uauf ••"„;,••,#, CK-^»-"^ '••••'
Sampling Location
Sample Type
Run Numbed -,,
Impinger Box Number
Rsoovajy Nfr&drt
Recovery Rinses
Sample Identmcatlon
Filter Number
XAD Number
L-W S\rd
U\acJ\^n
lo\^
lKc,\oi5
a
»rvlef
3&u3,U
Jx O-\b Ato03
U\/
UA
Impinger
Number
1
2
3
4
5
6
7
Impinger V
Solution i
^Ar
B*lo HM03
lO'/oUiOi
5% tt«OO3
IO% HzO2
Mr
M^oKMnCM
»0>0 H^cx,
M% KMoOq
IO& Hz So<(
^MliOv
GaJ
Amount of
Solution
(g)
-MOOq
^-,00^
.
^ lOOq
a
'"lOon
0
-ZWj
impiriger tlj^
dohffg'Ur'dtloh
Ko
M^5
GS
6s.
MGS
GS
G8
Impinger Weight _x ,
Final
(9)
MTI.M
LP ^M.-Z-
Bo-s,^
Mzn.c)
^sn.s
Biif-o
iZtb
Initial
(g)
.MSM.5
'1 ° -i -
•it) f • \j
5°»P.H
SOU. 8
^i^-.i
6-?o. S
57fa,Z.
"718, '5
Total Weight Gain (g)
Weight
Gain
(y)
'-(3 1
Hi. V
1 1
o.t
-o,>
-0. L
/o,3
in-6
-------
Eastern Reseirch Group. Inc
MODIFIED METHOD 5 DATASHEET
i Page : cf
Plant
Date
Ocerator
Sampling Location
Sample Type
Run Number
Static Pressure (±) (in. H2O)
•Barometric Pressure (in. H2O)
L,~Tv JXAD Trap_Number
{ „- -5.~?J7T| Filter Heater Setting (°F)
•viu/w ~pLv"l Probe Length & Type
-r^Me r
Probe Heater Settinq (°F)
fy>. <£V" (\(-S> \ Minimum Sample Volume (ft3)
3 | Initial Leak Check
— $.(e'( | Final Leak Check
^j^/
""^" I Meter Box Numoer
2-^ -
i>'uj*£S
i5>&
—
1 06 (^'C
, c^O/lSS*^'
Meter delta H @
DGM Factor (Y)
Nozzle Type & ID (in.)
Ambient Temperature (°F)
Assumed Moisture (% H2O)
K-Factor
t-w,_
, .-**,
."^^-^
^ -LO 3
fed '
/• <>
(d- *
Oi 05
-------
Eotfem RaMorch Group, he.
MOISTURE RECOVERY FORM FOR METHOD 4
\j '^
'\ \
Sampling Location
Samite Type f
Implnger Box Number
Recover WndǤ
Sample IdentiflcaUon
L i v
XAD Number
10 f\
'":. ' :• "•-; . . ''
Impinger
NiimBif ;
....:•• .;.• ••;:,:.,: '.:$....••.:
1
2
3
4
5
6
7
Impinger
Solution
MT
B"^ r^Oj
Vo'^o V\?0z
fJ?0v\uo3
lC/70 ^ttJ^
Kr
^^[) y>K<>oH
lo:l Mr y^
H^oK^'vOu
lo^ v\<^(
SiV..'^
G*<
Amount of
Solution
(g)
—
-«- >oO-x
^ >uo--x
(I
—
^ too<-
d^
^ ^oo-
; "
' zs"d
ImplrigerTip
Configuration
Ko
MG5
Gs
GS
M^GS
^S
Gs
Impinger Weig
Final
(g)
^')-*>- \
o^n-M
5^^ .7,
H1T7
G3i,>
5^2- ^
7^i).O
initial
(g)
U^^-V
G^o.^
6r\-i <
Ms 7.5
(fio.^
5tz.^
nio.>
Total Weight Gain (g)
ht; $&x>&s
^We^ht;
Gain
(gi ,
H>-J
?4,-^
-2. 1
0-2
o.£
- 0. i
S^
°/fe -^
-------
feERG
Eaton Research Group, loc.
Preliminary Velocity Traverse Fourm and Cyclonic Flow Check
Plant
Date
Location
Stack ID (In)
Barometric Pressure (in Hg)
Ambient Temperature (°F)
Static Pressure (in H2O)
Operators
Checked By
! C.*gr Cw > c
/(JO*
Schematic of Traverse Point Layout
(Cross Section of Duct)
Traverse
Point
Number
0- 1
-fr--T~
r>-3
c - 1
i
3
G-i
G-~z
<3-^
A- /
~L
3
Velocity
Head
AP, (in H2O)
2-3
/•£
1^
2.--L
'•1
2.9
2.q
2^6
^ H
2-1
7 -1
s.q
ITJ^O - 1 3
Stack
Temperature
Ts, (°F)
l^q
XS9
^MO
1V^
^-^
2Y^
^M^
2^9
aU-(<5
^•aO
Z^O
Z^(
:?o
Cyclonic
Flow
Angle (± °)
O '
O "
O *
o'
0 '
0'
0'
Ik °
0°
0 °
0 °
0°
Traverse
Point
Number
Velocity
Head
AP, (in H2O)
Stack
Temperature
Ts. (°F)
Cyclonic
Flow
Angle (± °)
Avernee of Absolute Values of All Ar !
r*""n mf t*
f A r^r»rf»'»f'lt Q-i mf\liM
-------
Eastern Research Group. Inc.
K-FACTOR CALCULATION FORM
Plant
Date
uv €,in o
Pb ± (stack static pressure (in. H^O) / 13.6)
HjO)
ii
Tf (average stack temperature, " R) = ~^> °
'F+ 460 = "R
Tm (average meter temperature, * R) = t&O "
Md (molecular weight of stack gas, dry, ib/lb-mole) =
(0.44 x %COj) + (032 x %Oj) + (0.28 x %N>)
Mg (molecular weight of
stack gas with water vapor,
Ib/lb-mole) =
K= (846.720)(Dn)4(A H@()(CD)2()-Bw)2(Md/Ms)(Ps/Pm)(Tm/Ts)
O.SV
ZJ^^fTT Q.H-3o
O . f 0J£
0'0&
^Q ^i/
J^W 1.3-9 1
^^ .«.to
7/L7
^-^•t) $"^-O
W.O
z^.?V
. d^L /) ^ (1
AH = KAP
Correlation Chart
1
AH
.t&M
,2_>6
iS6fr
AP
2-0
3-0
1--Q
2
AH
-
AP
3
AH
AP
Comments:
-------
Traverse Point Location Ftn m
Eastern Retaaich Group. Inc.
lant
late
ampling Location
btai Duct Depth (Distance A)
nside Far Wall to Outside of Nipple/Port) c V
Co
Upple/Port Length (Distance B) | H"
Inside Near Wall to Outside End of Nipple/Port)
itack Depth (Dist A - Dist B) [ Co"'
itack Width (If rectangular)
learest Upstream Disturbance
learest Downstream Disturbance
Sample Ports
Information
Number
I.D. (in)
Schematic of Sampling Location
(Cross Section of Duct)
1
Traverse
Point
Number
1tfcD 1
^
'2
>
2
Percent Fraction
of Stack ID
-/6-6V-
Cr, S'd
•0,1*-
3
Stack
ID
(in)
fell"
4
Product of Columns
2&3
(to nearest 1/8 inch)
/o''
z* "
£ 0 "
5
Distance
B
(in)
y"
Y"
y "
6
Traverse Point Location
from Outside of Nipple
(sum of columns 4 & 5)
W"
3V
SY"
-------
-------
Appendix E.2
Meter Box Calibrations
cah/K.\7997\03\07-RPT\APX-CVR WP6
-------
-------
. INSTRUMENTS
X METHOD 5
rfeter Box Pre-Test Calibration
English Meter Box and English Calibration Meter Units
/V
Fil
Model Nueber:
Serial Nuabar:
F:\0ATAFILE\CALIBRAT\CAL_MENU.DSK\DGK_PREL.5P\A-38.W1C1
511
A-38
Date:
Barometric Pressure:
Calibration Meter Factor Yc:
->4/29/97
•> 29.53 (in. Hg)
-> 1.0023 (nunber)
DRY GAS METER READING
Etaaped Volune Volume Volune
dH Time Initial Final Total
(in H20) (din) (cu ft) (cu ft) (cu ft)
5.00 10.00 212.123 224.631 12.508
3.00 12.50 224.631 236.780 12.149
2.00 10.00 236.780 244.791 8.011
1.00 22.00 244.791 257.487 12.696
0.50 14.00 257.487 263.361 5.874
GAS
Taaperature
Inlet Outlet
(deg F) (deg F)
79.0
87.0
81.0
82.0
81.0
91.0
85.0
85.0
83.0
85.0
69.0
74.0
73.0
75.0
75.0
76.0
74.0
77.0
78.0
78.0
CALIBRATION METER READINGS CALIBRATION METER
Volune Volume Volume Temperature
Initial Final Total Inlet Outlet
(cu ft) (cu ft) (cu ft) (deg F) (deg F)
82.098 94.425 12.327 71.0 71.0
94.425 106.269 11.844 71.0 71.0
106.269 114.045 7.776 71.0 71.0
114.045 126.309 12.264 71.0 71.0
126.309 131.965 5.656 71.0 71.0
Average
DRY GAS METER
METER CALIBRATION FACTOR
Y
Value Variation
(nunber) (nuttier)
0.987 0.003
0.982 -0.002
0.986 0.002
0.983 -0.001
0.982 -0.002
0.984
DRY GAS METER
ORIFICE CALIBRATION FACTOR
dK8
Value Variation
(in H20) (in H20)
1.865 0.038
1.885 0.058
1.861 0.033
1.811 -0.017
1.716 -0.112
Average 1.828
te: For Calibration Factor Y, the ratio of the reading of the calibration meter to the dry gas meter,
acceptable tolerance of individual value* from the average is *-0.02.
For Orifice Calibration Factor dH8, the orifice differential preaaure In Inches of H20 that equates to 0.75 cfm of air
at 68 F and 29.92 inches of Hg, acceptable tolerance of Individual values from the average la +-0.2.
sertify that the above Dry Gaa Meter was calibrated in accordance with E.P.A. Method 5 , paragraph 7.1 ;CFR 40 Part 60.
ng the Pracialon Wet Test Meter « 11AE6, which in turn Mas calibrated using the American Bell Prover * 3785,
tiflcate i F107, which is traceable to the National Bureau of Standard* (N.I.S.T.).
Signature
Date
-------
English Mater Box and English Calibration Meter Units
Filename: F:\DATAF1LE\CALIBRAT\CAL_MENU.DSK\DGM_PREL.5P\A-39.WK1
Model timber:
Serial Nunber:
511
A-39
Date:
Barometric Pressure:
Calibration Meter Factor Yc:
->4/30/97
-» 29.65 (In. Hg)
-> 1.0023 (nunfcer)
DRY GAS METER READING
Elasped Volune Volume Volume
dH Tine Initial Final Total
(in H20) (win) (cu ft) (cu ft) (cu ft)
GAS CALIBRATION METER READINGS CALIBRATION METER
Temperature Volume VoluM Volume Temperature
Inlet Outlet Initial Final Total Inlet Outlet
(deg F) (deg F) (cu ft) (cu ft) (cu ft) (deg F) (deg F)
5.00 6.00 117.896 125.546 7.650 Inftial-> 96.0 77.0 159.982 167.562 7.580 75.0 75.0
Flnal---> 98.0 79.0
3.00 32.50 125.546 158.483 32.937 lnit!al-> 93.0 79.0 167.562 199.789 32.227 75.0 75.0
Final---> 102.0 83.0
2.00 56.00 158.483 205.872 47.389 lnltlal-> 97.0 83.0 199.789 245.655 45.866 75.0 75.0
Final---> 102.0 86.0
1.00 22.00 205.872 218.935 13.063 In(tial-> 98.0 86.0 245.655 258.225 12.570 75.0 75.0
Final---> 98.0 85.0
0.50 15.00 251.983 258.408 6.425 Inltlal-> 87.0 83.0 290.051 296.269 6.218 75.0 75.0
Fln«l---> 94.0 83.0
DRY GAS METER
METER CALIBRATION FACTOR
Y
Value Variation
(number) (number)
DRY GAS METER
ORIFICE CALIBRATION FACTOR
dN3
Value Variation
(in H20) (In H20)
1.004 0.008
0.999 0.003
0.996 0.000
0.992 -0.004
0.990 -0.006
.774
.718
.668
.711
.632
0.073
0.017
-0.033
0.010
-0.068
Average
0.996
Average 1.700
Note: For Calibration Factor Y, the ratio of the reading of the calibration Meter to the dry gas meter,
acceptable tolerance of Individual values from the average Is *-0.02.
For Orifice Calibration Factor dH3, the orifice differential pressure In Inches of H20 that equates to 0.75 cfm of air
at 68 F and 29.92 Inches of Hg, acceptable tolerance of individual value* from the average Is +-0.2.
-------
Filename:
F:\DATAFILE\CALIBRAT\CAL_MENU.DSIC\DGM_PREL.5P\A-40.yiC1
Model Number:
Serial Number:
511
A-40
Date:
Barometric Pressure:
Calibration Meter Factor Yc:
->4/29/97
-> 29.58 (in. Hg)
-> 1.0023 (nuMber)
DRY GAS METER READING
Elasped Volune Volume Volume
dH . Time Initial Final Total
(in H20) (win) (cu ft) (cu ft) (cu ft)
GAS CALIBRATION METER READINGS CALIBRATION METER
Temperature Volume Volume Volume Temperature
Inlet Outlet Initial Final Total Inlet Outlet
(deg F) (deg F) (cu ft) (cu ft) (cu ft) (deg F) (deg F)
46.005 52.125 6.120 71.0 71.0
71.0 71.0
71.0 71.0
98.923 104.529 5.606
5.00 5.00 179.628 185.954 6.326 Initial-> 92.0 76.0
Final---> 96.0 79.0
3.00 14.00 209.020 223.316 14.296 Initial-> 94.0 82.0 74.309 87.941 13.632
Final---> 102.0 84.0
2.00 14.00 223.316 234.850 11.534 Initials 92.0 84.0 87.941 98.923 10.982
Final---> 96.0 85.0
1.00 10.00 234.850 240.728 5.878 Initial-> 89.0 84.0
Final---> 97.0 83.0
0.50 77.50 240.728 272.716 31.988 Initial-> 91.0 84.0 104.529 135.078 30.549 71.0 71.0
Final — -> 91.0 84.0
71.0 71.0
DRY GAS METER
METER CALIBRATION FACTOR
Y
Value Variation
(number) (number)
0.984 0.000
0.984 -0.001
0.982 -0.002
0.985 0.000
0.986 0.002
DRY GAS METER
ORIFICE CALIBRATION FACTOR
dxa
Value Variation
(in H20) (in H20)
.868 0.076
.753 -0.038
.795 0.004
.761 -0.030
.779 -0.012
Average 0.984
Average 1.791
Mote: For Calibration Factor Y, the ratio of the reading of the calibration meter to the dry gas meter,
acceptable tolerance of individual values from the average is +-0.02.
For Orifice Calibration Factor dH8, the orifice differential pressure in inches of H20 that equates to 0.75 cfw of air
at 68 F and 29.92 inches of Hg, acceptable tolerance of individual values from the average is +-0.2.
I certify that the above Dry Gas Meter was calibrated in accordance with E.P.A. Method 5 , paragraph 7.1 ;CFR 40 Part 60.
using the Precision Wet Test Meter * 11AE6, which in turn was calibrated using the American Bell Prm/i»r #
-------
'Y
^
\
APEX INSTRUMENTS
EPA METHOD 5
Meter Box Pre-Test Calibration
English Meter Box and English Calibration Meter Units
Filename: F:\DATAFILE\CALIBRAT\CAL_NENU.DSK\DGM_PREL.5P\A-35.UK1
Model Nuaber: 511 Date: ->4/25/97
Serial Nuaber: A-35 Baroaetrlc Pressure: •> 29.72 (in. Hg)
Calibration Neter Factor Yc: -> 1.0023 (nuaber)
DRY GAS METER READING GAS CALIBRATION METER READINGS CALIBRATION METER
Elaeped Voluae VoluM Voluat Teaperature voluae Voluaa Voluae Teeperature
dH Tia* Initial Final Total Inlet Outlet Initial Final Total Inlet Outlet
(in H20) (Bin) (cu ft) (cu ft) (cu ft) (deg F) (deg F) (cu ft) (cu ft) (cu ft) (deg F) (deg F)
5.00 25.00 642.638 672.722 30.084 Initial-> 79.0 73.0 839.501 869.250 29.749 71.0 71.0
Final---> 109.0 82.0
3.00 8.50 672.722 680.737 8.015 Init1al-> 98.0 82.0 869.250 877.161 7.911 71.0 71.0
Final--> 105.0 83.0
2.00 12.00 680.737 690.098 9.361 Initial-> 88.0 82.0 877.161 886.170 9.009 71.0 71.0
Final---> 102.0 82.0
1.00 13.00 690.098 697.456 7.358 Initial-> 96.0 82.0 886.170 893.289 7.119 71.0 71.0
Final---> 102.0 83.0
0.50 34.50 697.456 711.090 13.634 Initial^ 92.0 83.0 893.289 906.385 13.096 71.0 71.0
Final---> 95.0 83.0
DRY GAS METER DRY GAS METER
NETER CALIBRATION FACTOR ORIFICE CALIBRATION FACTOR
Y dH8
Value Variation Value Variation
(nuaber) (number) (in H20) (in H20)
1.006 0.003 1.967 0.048
1.021 0.018 1.911 -0.007
0.991 -0.011 1.960 0.042
1.003 0.000 1.840 -0.078
0.993 -0.010 1.913 -0.005
Average 1.003 Average 1.918
Note: For Calibration Factor Y, the ratio of the reading of the calibration Mter to the dry gas meter,
acceptable tolerance of individual values fraa the average is +-0.02.
For Orifice Calibration Factor dH3, the orifice differential pressure in inches of H20 that equates to 0.75 cfm of a
at 68 F and 29.92 inches of Hg, acceptable tolerance of individual values fro* the average is +-0.2.
I certify that the above Dry Gas Meter was calibrated in accordance with E.P.A. Method 5 , paragraph 7.1 ;CFR 40 Part 60,
using the Precision Wet 'Test Meter f 11AE6, which in turn was calibrated using the American Bell Prover * 3785,
certificate f F107, which is traceable to the National Bureau of Standards (N.I.S.T.).
Signature ^ - _ Date
-------
INSTRUMENTS
EPA METHOD 5
Neter Box Pre-Test Calibration
English Meter Box and English Calibration Neter Units
Fil
Model Number:
Serial Number:
F:\DATAFILE\CALIBRAT\CAL_M6MU.OSK\DGH_PREL.5P\A-36.WK1
511
A-36
Date:
Barometric Pressure:
Calibration Neter Factor Yc:
->4/25/97
•> 29.85 (in. Hg)
-> 1.0023 (renter)
DRY GAS METER READING
Elasped Volune Volume Volute
dH Tine Initial Final Total
(in H20) (Bin) (cu ft) (cu ft) (cu ft)
GAS
Temperature
Inlet Outlet
(deg F) (deg F)
CALIBRATION METER READINGS
Volune Volume Volune
Initial Final Total
(cu ft) (cu ft) (cu ft)
CALIBRATION METER
Temperature
Inlet Outlet
(deg F) (deg F)
5.00 7.50 537.187 546.733 9.546 Initial-> 102.0
Final---> 99.0
3.00 8.00 546.733 554.791 8.058 Initial-> 97.0
Final--->
Initial->
2.00 13.50 554.791 566.063 11.272
1.00 26.50 566.063 581.916 15.853
0.50 23.50 581.916 592.035 10.119
99.0
97.0
Final---> 104.0
Initial-> 97.0
Final---> 93.0
Initial-> 85.0
Final— > 98.0
73.0
76.0
77.0
78.0
79.0
81.0
81.0
82.0
82.0
82.0
919.384 928.649 9.265
928.649 936.419 7.770
936.419 947.225 10.806
947.225 962.350 15.125
962.350 972.000 9.650
71.0 71.0
71.0 71.0
71.0 71.0
71.0 70.0
70.0 70.0
DRY GAS METER
METER CALIBRATION FACTOR
Y
Value Variation
(number) (number)
DRY GAS METER
ORIFICE CALIBRATION FACTOR
dH3
Value Variation
(in H20) (in H20)
0.991 0.002
0.990 0.001
0.991 0.002
0.986 -0.003
0.985 -0.004
1.827
1.764
1.723
1.687
1.625
0.102
0.039
-0.002
-0.038
-0.100
Average
0.988
Average 1.725
Note: For Calibration Factor Y, the ratio of th« reading of the calibration meter to the dry gas meter,
acceptable tolerance of individual values from the average is +-0.02.
For Orifice Calibration Factor dH8, the orifice differential pressure in inches of H20 that equates to 0.75 cfm of air
at 68 F and 29.92 inches of Hg, acceptable tolerance of individual values from the average is +-0.2.
I certify that the above Dry Gas Meter was calibrated in accordance with E.P.A. Method 5 , paragraph 7.1 ;CFR 40 Part 60,
using the Precision Wet Test Meter * 11AE6, which in turn was calibrated using the American Bell Prover * 3785,
certificate * F107, which, is traceable to the National Bureau of Standards (N.I.S.T.).
Signature
IJ
Date
-------
'IMTWNEVTS
5
_ Bo* Pre-Test Calibration
tlsh Neter Box and English Calibration Meter Units
Model Nuaber:
Serial NtMber:
F:\DATAFILE\CALIBRAT\CAL_MENU.DSK\DGM_PREL.5P\A-37.UIC1
511
A-37
Date:
BaroMetric Pressure:
Calibration Neter Factor Yc:
•>4/30/97
•> 29.60 (in. Hg)
-> 1.0023 (nuifcer)
DRY GAS METER READING
Elasped VoluM Voluae Voline
dN TiMe
Initial Final Total
(in H20) (Min) (cu ft) (cu ft) (cu ft)
5.00 5.50 284.526 291.511 6.985
3.00 7.00 396.245 403.206 6.961
2.00 20.50 403.206 419.962 16.756
1.00 66.50 419.962 458.867 38.905
0.50 47.50 458.867 479.371 20.504
GAS CALIBRATION NETER READINGS CALIBRATION METER
Temperature Voluae Voluae Voluae Temperature
Inlet Outlet Initial Final Total Inlet Outlet
(deg F) (deg F) (cu ft) (cu ft) (cu ft) (deg F) (deg F)
Initial->
Final--->
Initial->
Final--->
Initial->
Final--->
Initial->
Finel--->
Im'tial->
Final--->
93.0
97.0
101.0
98.0
93.0
98.0
93.0
98.0
94.0
91.0
81.0
82.0
80.0
81.0
79.0
82.0
82.0
86.0
86.0
87.0
309.486
419.901
426.763
443.220
481.231
316.381
426.763
443.220
481.231
501.111
6.895
6.862
16.457
38.011
19.880
76.0
76.0
77.0
77.0
77.0
76.0
77.0
77.0
77.0
78.0
DRY GAS METER
METER CALIBRATION FACTOR
Y
Value Variation
(timber) (nuaber)
DRY GAS METER
ORIFICE CALIBRATION FACTOR
dxa
Value Variation
(in H20) (in H20)
1.000 0.000
1.005 0.006
1.000 0.000
1.000 0.001
0.992 -0.007
1.799
1.772
1.765
1.730
1.609
0.064
0.037
0.030
-0.005
-0.126
Average 0.999
Average 1.735
Note: For Calibration Factor Y, the ratio of the reading of the calibration Meter to the dry gas Meter,
acceptable tolerance of individual values fro» the average is +-0.02.
For Orifice Calibration Factor dH8. the orifice differential pressure In inches of H20 that equates to 0.75 cfm of air
at 68 F and 29.92 inches of Hg, acceptable tolerance of individual values fro* the average is +-0.2.
I certify that the above Dry Gas Meter was calibrated in accordance uith E.P.A. Method 5 , paragraph 7.1 ;CFR 40 Part 60,
using the Precision Wet Test Meter f 11AE6, which in turn was calibrated using the American Bell Prover f 3785,
certificate f F107, which is traceable to the National Bureau of Standards (N.I.S.T.).
Signature
Date
-------
Box Post-Test Calibration
'Filename:
Model Number:
Serial Number:
F:\DATAFILE\CALIBRAT\CALJIENU.DSIC\DGM_POST.3P\A-38P.WIC1
511
A-38
Date:
Barometric Pressure:
Calibration Meter Factor Yc:
•>7/2/97
-> 29.55 (in. Hg)
-> 1.0023 (number)
I'
f ~\
- ,'
DRY GAS METER READING
Elasped Volume Volume Volume
dH Time Initial Final Total
;in H20) (min) (cu ft) (cu ft) (cu ft)
0.83 12.00 814.652 821.068 6.416 Initial-> 98.0 87.0 617.479 623.625 6.146
Final---> 98.0 88.0
0.83 9.50 821.068 826.157 5.089 Initial-> 98.0 88.0 623.625 628.509 4.884
Final---> 97.0 88.0
0.83 72.50 826.157 865.235 39.078 Initial-> 95.0 83.0 628.509 665.789 37.280
Final---> 96.0 86.0
GAS CALIBRATION METER READINGS CALIBRATION METER
Temperature Volume Volume Volume Temperature
Inlet Outlet Initial Final Total Inlet Outlet
(deg F> (deg F) (cu ft) (cu ft) (cu ft) (deg F) (deg F)
84.0 84.0
84.0 84.0
84.Q 84.0
Average
DRY GAS METER
METER CALIBRATION FACTOR
Y
Value Variation
(number) (number)
0.974 0.002
0.975 0.004
0.965 -0.006
0.971
DRY GAS METER
ORIFICE CALIBRATION FACTOR
dHS
Value Variation
(in H20) (in H20)
1.826 0.007
1.811 -0.009
1.822 0.002
Average 1.820
te: For Calibration Factor Y, the ratio of the reading of the calibration meter to the dry gas meter,
acceptable tolerance of individual values from the average is +-0.02.
For Orifice Calibration Factor dH3. the orifice differential pressure in inches of H20 that equates to 0.75 cfm of air
at 68 F and 29.92 inches of Hg, acceptable tolerance of individual values from the average is +-0.2.
ertify that the above Dry Gas Meter was calibrated in accordance with E.P.A. Method 5 , paragraph 7.1 ;CFR 40 Part 60.
ng the Precision Wet Test Meter # 11AE6, which in turn was calibrated using the American Bell Prover # 3785,
tificate # F107, which is traceable to the National Bureau of Standards (N.I.S.T.).
Signature
Date
-------
APEX INSTRUMENTS
EPA METHOD 5 .
Meter Box Post-Test Calibration
English Meter Box and English Calibration Meter Units
Filename:
F:\DATAFILE\CALIBRAT\CAL_NENU.DSK\DGM_POST.3P\A-39P.WIC1
Model Number: 511
Serial Nunber: A-39
Date:
Barometric Pressure:
Calibration Meter Factor Yc:
->7/2/97
-> 29.55 (in. Hg)
-> 1.0023 (number)
DRY GAS METER READING
Elasped Volume Volume Volume
dH Time Initial Final Total
(in H20) (min) (cu ft) (cu ft) (cu ft)
GAS CALIBRATION METER READINGS CALIBRATION METER
Teaperature Volume Volume Volume Temperature
Inlet Outlet Initial Final Total Inlet Outlet
(deg F) (deg F) (cu ft) (cu ft) (cu ft) (deg F) (deg F)
0.82 10.50 754.507 760.029 5.522 Initial-> 82.0 75.0 533.834 539.225 5.391 85.0 85.0
Final---> 89.0 78.0
0.82 14.00 760.029 767.123 7.094 Initial-> 86.0 78.0 539.225 546.108 6.883 85.0 85.0
Final---> 94.0 81.0
0.82 18.00 776.115 785.136 9.021 Initial-> 85.0 83.0 554.795 563.509 8.714 85.0 85.0
Final---> 98.0 83.0
DRY GAS HETER
METER CALIBRATION FACTOR
Y
Value Variation
(number) (number)
DRY GAS METER
ORIFICE CALIBRATION FACTOR
dH3
Value Variation
(in H20) (in H20)
0.969 -0.001
0.970 0.000
0.970 0.000
1.839 -0.120
1.994 0.035
2.044 0.085
Average 0.970
Average 1.959
Note: For Calibration Factor Y, the ratio of the reading of the calibration meter to the dry gas meter,
acceptable tolerance of individual values from the average is +-0.02.
For Orifice Calibration Factor dHS, the orifice differential pressure in inches of H20 that equates to 0.75 cfm of air
at 68 F and 29.92 inches of Hg, acceptable tolerance of individual values from the average is +-0.2.
I certify that the above Dry Gas Meter was calibrated in accordance with E.P.A. Method 5 , paragraph 7.1 ;CFR 40 Part 60,
using the Precision Wet Test Meter # 11AE6, which in turn was calibrated using the American Bell Proven # 3785,
certificate * F107, which is traceable to the National Bureau of Standards (N.I.S.T.).
Signature
I
Date
-------
OCT-ffii-1997 10:10 AFEX INSTRUMENTS 919 557 7UQ p.01
f
APE* IHSWJUENTS
EM NETNUD i
fht«T Box P.i*t-Te«t Calibration
Eretiah Met-if «ox and Enaliah Calibration Meter Units
FlUnMM! F:\0ATAme\CAUBRAT\CAl JW«J.DSK\D«J>9ST.3P\A-40.WK1
Hcd« I Nunba •! 511 Data:
Sariial «II*M : A-40P Barometric Pressures •> 29.55 (fn. Hg)
Calibration Meter Factor Yc: -> 1.0023 (nuaber)
MY flAS METER BEAD INC GAS CALIBRATION METER READINGS CAL1MATIOM METER
El.isp#d Volum VoluM Volume Temperature Volume volume Volume Teaperature
o,H Tine Initial final Total Inlet Outlet Initial final Total inlet outlet
(It H20) <»n) (cu ft) (cu ft) (cu ft) (de* F) 104.0 66.0
1.65 1..M Ml.677 551.737 10.060 Jnitlal-» 95.0 86.0 702.661 712.322 9.661 94.0 84.0
final---* 101.0 87.0
DRY GAS METER DRY GAS METER
lUETER CALIBRATION FACTOR ORIFICE CALIBRATION FACTOR
Value Variation Value Variation
(nuifcar)
-------
APEX INSTRUMENTS 623 SERIES METER CONSOLE CALIBRATION
Meter Console Information
Console Model Number
Gas Meter Model
Totalizer Model
Temp Controller Model
623
Kimmon PK-III
Durant 53300-403
Watlow 935
Console Serial Number
Gas Meter Serial Number
Totalizer Scale Factor
High Flow Orifice Model
707010
707010
3.52750
55
Manufacture Date
Encoder Model
Temp Display Model
Low Flow Orifice Model
29-May-97
HP HEDS-5701-A02
Watlow 935
33
Wet Test Meter Idenification
Wet Test Meter Calibration Factor
Calibration Conditions
11AE6
1.0003
Calibration Technician
Barometric Pressure
VHJ
(Pb)
754.0
Calibration Date |29-May-97
mm Hg I
Version Number
2.0 [Last Update
Calibration Worksheet Information
| 09-Jan-97 [Filename | C:\DATAFILE\CALIBRAT\DGM_6005.PR5\707010.XLS
Run 1 - Initial
Final
Total/Avg
Run 2 - Initial
Final
Total/Avg
Run 3 • Initial
Final
Total/Avg
Run 4 - Initial
Final
Total/Avg
Run 5 - Initial
Final
TotaUAvg
Run 6 - Initial
Final
Total/Avg
Calibration Data
Run Time
Elapsed
(9)
mm
5.50
5.50
5.50
0.00
14.00
14.00
13.00
13.00
13.00
6.00
6.00
6.00
6.50
6.50
6.50
21.00
21.00
21.00
Orifice
Number
55
55
55
55
55
55
55
55
55
33
33
33
33
33
33
33
33
33
Dry Oas Meter
Oas
Pressure
(Pm)
mm H2O
20.0
20.0
20.0
25.0
25.0
25.0
40.0
40.0
40.0
80.0
80.0
80.0
60.0
600
60.0
25.0
25.0
250
Oas
Volume
(V™)
liters
0.000
7.093
7.093
0.000
18.999
18.999
0.000
23.785
23.785
0.000
6.666
6.666
0.000
6.857
6.857
0.000
11.922
11.922
Oas
Temperature
(U
°c
29
29
29
29
29
29
29
29
29
27
28
28
28
28
28
28
30
30
Wet Test Meter
Oas
Volume
(V,)
liters
0.000
7.040
7.040
0.000
18.800
18.800
0.000
23.380
23.380
0.000
6.650
6.650
0.000
6.880
6.880
0.000
12.100
12.100
Gas
Temperature
(U)
°C
25
25
25
25
25
25
25
26
26
26
26
26
26
26
26
26 I
27
27
Results
Standardized Volumes
Dry Gas
Meter
(V**!))
std liters
Wet Test
)
std liters
Dry Qas Meter
Calibration Factor
Value
00
Variation
(AY)
Corrected
Ftewrate
(CW
slm
6.845
6874
1.004
0.001
1.25
18.345
18.357
1.001
-0.003
1.31
23000
22.753
0.989
-0.014
1.75
6.492
6.472
0.997
-0.007
1.08
6.666
6.695
1.004
0.001
1.03
11.474
11.756
1.025
0.021
0.56
Average Meter Calibration Factor Y 1 1.003 |
|nol». For Calibration Factor Y. the ratio of the reading of the calibration meter to the dry gas meter, acceptable tolerance of individual values from the averape is +-0.02. ~|
r that the above Dry Gas Meter was calibrated in accordance with USEPA Methods, CFR 40 Part 60, using the Precision Wet Test Meter # 11AE6,
yrUum was calibrated using the American Bell Prover # 3785, certificate # F107, which is traceable to the National Bureau of Standards (N.I.S.T.).
-------
APEX INSTRUMENTS 623 SERIES METER CONSOLE CALIBRATION
f
Meter Console Information
Console Model Number
Gas Meter Model
Totalizer Model
Temp Controller Model
623
Kimmon PK-III
Durant 53300-403
Watlow 935
Console Serial Number
Gas Meter Serial Number
Totalizer Scale Factor
High Flow Orifice Model
702004
702004
340000
55
Manufacture Date
Encoder Model
Temp Display Model
Low Flow Orifice Model
30-Jan-97
HPHEDS-5701-A02
Watlow 935
33
Calibration Conditions
Wet Test Meter Idenification
Wet Test Meter Calibration Factor
11AE6
1.0003
Calibration Technician
Barometric Pressure
VHJ
fPb)
758,0
Calibration Date
01-Jul-97
mm Hg I
Version Number
2 0 Last Update
Calibration Worksheet Information
| 09-Jan-97 [Filename"
C:\DATAFILE\CALIBRAT\DGM 6005.PR5\702004.XLS
Run 1 - Initial
Final
Total/Avg
Run 2 - Initial
Final
Total/Avg
Run 3 - Initial
Final
Total/Avg
Run 4 - Initial
Final
Total/Avg
60.00
Final
Total/Avg
Run 6 - Initial
Final
Total/Avg
Calibration Data
Run Time
Elapsed
(9)
mm
500
500
5.00
600
6.00
6.00
10.50
10.50
10.50
7.50
750
7.50
9.50
9.50
9.50
1000
10.00
1000
Orifice
Number
55
55
55
55
55
55
55
55
55
33
33
33
33
33
33
33
33
33
Dry Gas Meter
Gas
Pressure
(Pm)
mm H2O
35.0
35.0
35.0
25.0
25.0
25.0
20.0
20.0
20.0
80.0
80.0
80.0
60.0
600
60.0
30.0
30.0
300
Gas
Volume
-------
-------
Appendix E.3
Chain-of-Custody Sheets
cah/K.\7997\03\07-RPT\APX-CVR.WP6
-------
-------
LTV STEEL COMPANY
CHAIN OF CUSTODY
RELINQUISHED BY'
RELINQUISHED BY'
A.
DATE'
DATE'
RECEIVED BY:.
RECEIVED BY:
DATE:.
DATE:
SAMPLE ID
LTV-94
LTV-103
LTV-95
LTV-102
LTV-104
LTV-105
LTV-106
LTV-107
LTV-108
FIELD ID
LTV- 062497- PROCESS- SINTER- TEST-
LTV- 062597- PROCESS- SINTER- 1
LTV- 062597- PROCESS- BLOW OUT- 1
LTV- 062697- PROCESS- MILL SCALE 2
LTV- 062697- PROCESS- BLOWOUT- 2
LTV- 062697- PROCESS- SINTER- 2
LTV- 062797- PROCESS- SINTER- 3
LTV- 062797- PROCESS- BLOW OUT- 3
LTV- 062797- PROCESS- MILL SCALE 3
SAMPLE TYPE
PROCESS, SINTER FEED, TEST DAY
PROCESS, SINTER FEED, RUN 1
PROCESS, SCRUBBER BLOW OUT, RUN 1
PROCESS, MILL SCALE, RUN 2
PROCESS, SCRUBBER BLOW OUT. RUN 2
PROCESS. SINTER FEED, RUN 2
PROCESS, SINTER FEED, RUN 3
PROCESS, SCRUBBER BLOW OUT, RUN 3
PROCESS, MILL SCALE, RUN 3
PRESERVATIVE
Sinter Feed
Sinter Feed
Scrubber Blow Out
Mill Scale
Scrubber Blow Out
Sinter Feed
Sinter Feed
Scrubber Blow Out
Mill Scale
COMMENTS
ANALYSIS
Hold
Hold
Hold
Hold
Hold
Hold
Hold
Hold
Hold
Page 1
-------
LTV STEEL COMPANY
CHAIN OF CUSTODY
RELINQUISHED BY =
RELINQUISHED BY =
DATE =
DATE =
o~
RECEIVED BY:.
RECEIVED BY:
DATE:.
DATE:
SAMPLE ID
LTV-03
LTV-21
LTV-09
LTV-27
LTV- 15
LTV-33
LTV-40
LTV-53
LTV-47
LTV-60
LTV-04
LTV-22
LTV-10
LTV-28
LTV-16
LTV-34
LTV-41
LTV-54
FIELD ID
LTV- 062497- M29- OUTLET- BH- 1
LTV- 062497- M29- INLET- BH- 1
LTV- 062697- M29- OUTLET- BH- 2
LTV- 062697- M29- INLET- BH- 2
LTV- 062797- M29- OUTLET- BH- 3
LTV- 062797- M29- INLET- BH- 3
LTV- 062697- M29- OUTLET- BH- FB1
LTV- 062697- M29- INLET- BH- FB2
LTV- 062497- M29- OUTLET- BH- RB1
LTV- 062597- M29- INLET- BH- RB2
LTV- 062497- M29- OUTLET- BHM- 1
LTV- 062497- M29- INLET- BHM- 1
LTV- 062697- M29- OUTLET- BHM- 2
LTV- 062697- M29- INLET- BHM- 2
LTV- 062797- M29- OUTLET- BHM- 3
LTV- 062797- M29- INLET- BHM- 3
LTV- 062697- M29- OUTLET- BHM- FBI
LTV- 062697- M29- INLET- BHM- FB2
SAMPLE TYPE
METHOD 29, OUTLET, RUN 1
METHOD 29, INLET, RUN 1
METHOD 29, OUTLET, RUN 2
METHOD 29, INLET, RUN 2
METHOD 29, OUTLET, RUN 3
METHOD 29, INLET, RUN 3
METHOD 29, OUTLET, FBI
METHOD 29, INLET, FB2
METHOD 29, OUTLET, RB1
METHOD 29, INLET, RB2
METHOD 29, OUTLET, RUN 1
METHOD 29, INLET, RUN 1
METHOD 29, OUTLET, RUN 2
METHOD 29, INLET, RUN 2
METHOD 29, OUTLET, RUN 3
METHOD 29, INLET, RUN 3
METHOD 29, OUTLET, FB1
METHOD 29, INLET, FB2
PRESERVATIVE
HNO3/H2O2 BACK HALF
HNO3/H2O2 BACK HALF
HNO3/H2O2 BACK HALF
HNO3/H2O2 BACK HALF
HNO3/H2O2 BACK HALF
HNO3/H202 BACK HALF
HNO3/H2O2 BACK HALF
HNO3/H2O2 BACK HALF
HNO3/H2O2
HNO3/H2O2
0.1 NHNO3 RINSE - Hg
0.1 NHN03 RINSE -Hg
0.1 NHNO3 RINSE -Hg
0 IN HNO3 RINSE - Hg
0.1 NHNO3 RINSE -Hg
0.1 NHNO3 RINSE -Hg
0.1 NHNO3 RINSE - Hg
0.1 NHNO3 RINSE - Hg
COMMENTS
ANALYSIS
Metals
Metals
Metals
Metals
Metals
Metals
Metals
Metals
Metals
Metals
Metals
Metals
Metals
Metals
Metals
Metals
Metals
Metals
Page3
-------
LTV STEEL COMPANY
CHAIN OF CUSTODY
RELINQUISHED BY'
RELINQUISHED BY'
DATE =
DATE'
RECEIVED BY:.
RECEIVED BY:
DATE:.
DATE:
SAMPLE ID
LTV-06
LTV-24
LTV-12
LTV-30
LTV-18
LTV-36
LTV-43
LTV-56
LTV-49
LTV-62
FIELD ID
LTV- 062497- M29- OUTLET- HCI- 1
LTV- 062497- M29- INLET- HCI- 1
LTV- 062697- M29- OUTLET- HCI- 2
LTV- 062697- M29- INLET- HCI- 2
LTV- 062797- M29- OUTLET- HCI- 3
LTV- 062797- M29- INLET- HCI- 3
LTV- 062697- M29- OUTLET- HCI- FB1
LTV- 062697- M29- INLET- HCI- FB2
LTV- 062497- M29- OUTLET- HCI- RB1
LTV- 062797- M29- INLET- HCI- RB2
SAMPLE TYPE
METHOD 29, OUTLET, RUN 1
METHOD 29, INLET, RUN 1
METHOD 29, OUTLET, RUN 2
METHOD 29, INLET, RUN 2
METHOD 29, OUTLET, RUN 3
METHOD 29, INLET, RUN 3
METHOD 29, OUTLET, FB1
METHOD 29, INLET, FB2
METHOD 29, OUTLET, RBI
METHOD 29, INLET, RB2
PRESERVATIVE
8N HCI RINSE - Hg
8N HCI RINSE - Hg
8N HCI RINSE - Hg
8N HCI RINSE - Hg
8N HCI RINSE - Hg
8N HCI RINSE - Hg
8N HCI RINSE - Hg
8N HCI RINSE - Hg
8NHCI
8NHCI
COMMENTS
ANALYSIS
Metals
Metals
Metals
Metals
Metals
Metals
Metals
Metals
Metals
Metals
PageS
-------
LTV STEEL COMPANY
CHAIN OF CUSTODY
RELINQUISHED BY'
RELINQUISHED BY'
DATE'
DATE'
I,
RECEIVED BY:.
RECEIVED BY:
DATE:.
DATE:
SAMPLE ID
LTV-02
LTV-20
LTV-101
LTV-08
LTV-26
LTV-14
LTV-32
LTV-38
LTV-51
LTV-96
LTV-97
LTV-45
LTV-58
FIELD ID
LTV- 062497- M29- OUTLET- HN- 1
LTV- 062497- M29- INLET- HN- 1
LTV- 062597- M29- INLET- HN- 1A
LTV- 062697- M29- OUTLET- HN- 2
LTV- 062697- M29- INLET- HN- 2
LTV- 062797- M29- OUTLET- HN- 3
LTV- 062797- M29- INLET- HN- 3
LTV- 062697- M29- OUTLET- HN- FB1
LTV- 062697- M29- INLET- HN- FB2
LTV- 062597- M29- OUTLET- HNO- PB
LTV- 062597- M29- INLET- HNO- PB
LTV- 062497- M29- OUTLET- HNO- RB1
LTV- 062697- M29- INLET- HNO- RB2
SAMPLE TYPE
METHOD 29, OUTLET, RUN 1
METHOD 29, INLET, RUN 1
METHOD 29, OUTLET, RUN 1
METHOD 29, OUTLET, RUN 2
METHOD 29, INLET, RUN 2
METHOD 29, OUTLET, RUN 3
METHOD 29, INLET, RUN 3
METHOD 29, OUTLET, FB1
METHOD 29, INLET, FB2
METHOD 29, OUTLET, PROOF BLANK
METHOD 29, INTLET, PROOF BLANK
METHOD 29, OUTLET, RB1
METHOD 29, INLET, RB2
PRESERVATIVE
NITRIC ACID PROBE RINSE
NITRIC ACID PROBE RINSE
Nitric Acid Probe Rinse
NITRIC ACID PROBE RINSE
NITRIC ACID PROBE RINSE
NITRIC ACID PROBE RINSE
NITRIC ACID PROBE RINSE
NITRIC ACID PROBE RINSE
NITRIC ACID PROBE RINSE
0.1NHNO3 Rinse
0.1 NHNO3 Rinse
0.1NHNO3
0.1NHNO3
COMMENTS
\V<
W
ANALYSIS
Metals
Metals
Metals
Metals
Metals
Metals
Metals
Metals
Metals
> li Metals""" L
>^ -MeldlsT *
Metals
Metals
Page 6
-------
LTV STEEL COMPANY
CHAIN OF CUSTODY
RELINQUISHED BY - O uJUs L-
RELINQUISHED BY =
DATE'
DATE'
RECEIVED BY:.
RECEIVED BY:
DATE:.
DATE:
SAMPLE ID
LTV-05
LTV-23
LTV-11
LTV-29
LTV-17
LTV-35
LTV-42
LTV-55
LTV-48
LTV-61
FIELD ID
LTV- 062497- M29- OUTLET- KMnO- 1
LTV- 062497- M29- - INLET- KMnO- 1
LTV- 062697- M29- OUTLET- KMnO- 2
LTV- 062697- M29- INLET- KMnO- 2
LTV- 062797- M29- OUTLET- KMnO- 3
LTV- 062797- M29- INLET- KMnO- 3
LTV- 062697- M29- OUTLET- KMnO- FB1
LTV- 062697- M29- INLET- KMnO- FB2
LTV- 062497- M29- OUTLET- KMnO- RB1
LTV- 062597- M29- INLET- KMnO- RB2
SAMPLE TYPE
METHOD 29, OUTLET, RUN 1
METHOD 29, INLET, RUN 1
METHOD 29, OUTLET, RUN 2
METHOD 29, INLET, RUN 2
METHOD 29, OUTLET, RUN 3
METHOD 29, INLET, RUN 3
METHOD 29. OUTLET, FB1
METHOD 29, INLET, FB2
METHOD 29, OUTLET, RB1
METHOD 29, INLET, RB2
PRESERVATIVE
KMn04 IMPINGERS
KMnO4 IMPINGERS
KMnO4 IMPINGERS
KMn04 IMPINGERS
KMnO4 IMPINGERS
KMnO4 IMPINGERS
KMnO4 IMPINGERS
KMnO4 IMPINGERS
KMnO4
KMnO4
COMMENTS
ANALYSIS
Metals
Metals
Metals
Metals
Metals
Metals
Metals
Metals
Metals
Metals
Page 7
-------
LTV STEEL COMPANY
CHAIN OF CUSTODY
RELINQUISHED BY'
RELINQUISHED BY'
L - 6
<^nJJ
DATE"
DATE =
RECEIVED BY:
RECEIVED BY:
DATE:
DATE:
SAMPLE ID
LTV-98
LTV-63
LTV-68
LTV-73
LTV-78
LTV-83
LTV-64
LTV-69
LTV-74
LTV-79
LTV-84
LTV-66
LTV-71
LTV-76
LTV-81
LTV-86
LTV-65
LTV-70
LTV-75
LTV-80
LTV-85
LTV-67
LTV-72
LTV-77
LTV-82
LTV-87
FIELD ID
LTV- 062597- M23- OUTLET- MeCI2- PB
LTV- 062497- M23- OUTLET- PR- 1
LTV- 062697- M23- OUTLET- PR- 2
LTV- 062797- M23- OUTLET- PR- 3
LTV- 062697- M23- OUTLET- PR- FB1
LTV- 062497- M23- OUTLET- PR- RB1
LTV- 062497- M23- OUTLET- PRT/CRT- 1
LTV- 062697- M23- OUTLET- PRT/CRT- 2
LTV- 062797- M23- OUTLET- PRT/CRT- 3
LTV- 062697- M23- OUTLET- PRT/CRT- FB1
LTV- 062497- M23- OUTLET- PRT/CRT- RB1
LTV- 062497- M23- OUTLET- XAD- 1
LTV- 062697- M23- OUTLET- XAD- 2
LTV- 062797- M23- OUTLET- XAD- 3
LTV- 062697- M23- OUTLET- XAD- FB1
LTV- 062497- M23- OUTLET- XAD- RB1
LTV- 062497- M23- OUTLET- F- 1
LTV- 062697- M23- OUTLET- F- 2
LTV- 062797- M23- OUTLET- F- 3
LTV- 062697- M23- OUTLET- F- FB1
LTV- 062497- M23- OUTLET- F- RB1
LTV- 062497- M23- OUTLET- IMP- 1
LTV- 062697- M23- OUTLET- IMP- 2
LTV- 062797- M23- OUTLET- IMP- 3
LTV- 062697- M23- OUTLET- IMP- FB1
LTV- 062497- M23- OUTLET- IMP- RB1
SAMPLE TYPE
METHOD 23, INLET, PROOF BLANK
METHOD 23, OUTLET, RUN 1
METHOD 23, OUTLET, RUN 2
METHOD 23, OUTLET, RUN 3
METHOD 23, OUTLET, FB 1
METHOD 23, OUTLET, RB 1
METHOD 23, OUTLET, RUN 1
METHOD 23, OUTLET, RUN 2
METHOD 23, OUTLET, RUN 3
METHOD 23, OUTLET, FB 1
METHOD 23, OUTLET, RB 1
METHOD 23, OUTLET, RUN 1
METHOD 23, OUTLET, RUN 2
METHOD 23, OUTLET, RUN 3
METHOD 23, OUTLET, FB 1
METHOD 23. OUTLET, RB 1
METHOD 23, OUTLET, RUN 1
METHOD 23, OUTLET, RUN 2
METHOD 23, OUTLET, RUN 3
METHOD 23, OUTLET, FB 1
METHOD 23, OUTLET. RB 1
METHOD 23. OUTLET, RUN 1
METHOD 23, OUTLET, RUN 2
METHOD 23, OUTLET, RUN 3
METHOD 23, OUTLET, FB 1
METHOD 23, OUTLET, RB 1
PRESERVATIVE
MeCI2 Rinse
MeCI2/Acetone Probe Rinse
MeCI2/Acetone Probe Rinse
MeCI2/Acetone Probe Rinse
MeCI2/Acetone Probe Rinse
MeCI2/Acetone Probe Rinse
Toluene Probe Rinse
Toluene Probe Rinse
Toluene Probe Rinse
Toluene Probe Rinse
Toluene Probe Rinse
XAD Trap
XAD Trap
XAD Trap
XAD Trap
XAD Trap
Filter
Fitter
Filter
Filter
Filter
Impingers and Rinses
Impingers and Rinses
Impingers and Rinses
Impingers and Rinses
Impingers and Rinses
COMMENTS
ANALYSIS
loiv,ii»/rAiic
Dioxins/PAH
Dioxins/PAH
Dioxins/PAH
Dioxins/PAH
Dioxins/PAH
Dioxins/PAH
Dioxins/PAH
Dioxins/PAH
Dioxins/PAH
Dioxins/PAH
Dioxins/PAH
Dioxins/PAH
Dioxins/PAH
Dioxins/PAH
Dioxins/PAH
Dioxins/PAH
Dioxins/PAH
Dioxins/PAH
Dioxins/PAH
Dioxins/PAH
Dioxins/PAH
Dioxins/PAH
Dioxins/PAH
Dioxins/PAH
Dioxins/PAH
PageS
-------
Appendix E.4
Summary of Sampling Parameters
cah/K.\7997\03\07-RPT\APX-CVR WP6
-------
-------
Facility:
Date:
Location:
Run Number:
Sample Tvoe:
LTV East Chicago
6/25/97
Inlet
1
Multi metals
Total Sampling Time (min)
Corrected Barometric Pressure (in Hg)
Absolute Stack Pressure (in H2O)
Stack Static Pressure (in H2O)
Average Stack Temperature (°F)
Stack Area (sq in)
Actual Meter Volume (cu ft)
Average Meter Pressure (in H2O)
Average Meter Temperature (°F)
Moisture Collected (g)
Carbon Dioxide Concentration (%V)
Oxygen Concentration (%V)
Nitrogen Concentration (%V)
Dry Gas Meter Factor
Nozzle Diameter (in)
Pitot Constant
Average Sampling Rate (dscfm)
Standard Metered Volume (dscf)
Standard Metered Volume (dscm)
Stack Moisture (%V)
Mole Fraction Dry Stack Gas
Dry Molecular Weight
Wet Molecular Weight
Stack Gas Velocity (fpm)
Stack Gas Velocity (mpm)
Volumetric Flow Rate, (acfm)
Volumetric Flow Rate (acmm)
Volumetric Flow Rate (dscfm)
Volumetric Flow Rate (dscmm)
Percent Isokinetic
Percent Excess Air
Concentration (g/dscm)
Concentration (kg/hr)
Concentration (ppmv)
Emissions (Ib/hr)
240.0
29.36
28.95
-5.60
222.04
8190.00
67.248
1.66
92.08
93.20
2.5
19.0
88.5
0.9840
0.103
0.84
0.259
62.194
1.761
6.60
0.934
31.96
31.04
6236.47
1900.88
354699.39
10045.09
248105.45
7026.35
102.66
433.62
0.00
0.00
0.00
0.00
-------
Facility:
Date:
Location:
Run Number:
Sample Type:
LTV East Chicago
6/26/97
Inlet
2
Multi metals
Total Sampling Time (min)
Corrected Barometric Pressure (in Hg)
Absolute Stack Pressure (in H2O)
Stack Static Pressure (in H2O)
Average Stack Temperature (°F)
Stack Area (sq in)
Actual Meter Volume (cu ft)
Average Meter Pressure (in H2O)
Average Meter Temperature (°F)
Moisture Collected (g)
Carbon Dioxide Concentration (%V)
Oxygen Concentration (%V)
Nitrogen Concentration (%V)
Dry Gas Meter Factor
Nozzle Diameter (in)
Pitot Constant
Average Sampling Rate (dscfm)
Standard Metered Volume (dscf)
Standard Metered Volume (dscm)
Stack Moisture (%V)
Mole Fraction Dry Stack Gas
Dry Molecular Weight
Wet Molecular Weight
Stack Gas Velocity (fpm)
Stack Gas Velocity (mpm)
Volumetric Flow Rate (acfm)
Volumetric Flow Rate (acmm)
Volumetric Flow Rate (dscfm)
Volumetric Flow Rate (dscmm)
Percent Isokinetic
Percent Excess Air
Concentration (g/dscm)
Concentration (kg/hr)
Concentration (ppmv)
Emissions (Ib/hr)
240.0
29.45
29.04
-5.60
222.63
8190.00
68.915
1.62
93.31
98.60
3.3
18.8
88.0
0.9840
0.103
0.84
0.266
63.785
1.806
6.79
0.932
32.07
31.11
6057.53
1846.33
344521.82
9756.86
241027.11
6825.89
108.38
416.70
0.00
0.00
0.00
0.00
-------
Facility:
Date:
Location:
Run Number:
Sample Type:
LTV East Chicago
6/27/97
Inlet
3
Multi metals
Total Sampling Time (min)
Corrected Barometric Pressure (in Hg)
Absolute Stack Pressure (in H2O)
Stack Static Pressure (in H2O)
Average Stack Temperature (°F)
Stack Area (sq in)
Actual Meter Volume (cu ft)
Average Meter Pressure (in H2O)
Average Meter Temperature (°F)
Moisture Collected (g)
Carbon Dioxide Concentration (%V)
Oxygen Concentration (%V)
Nitrogen Concentration (%V)
Dry Gas Meter Factor
Nozzle Diameter (in)
Pitot Constant
Average Sampling Rate (dscfm)
Standard Metered Volume (dscf)
Standard Metered Volume (dscm)
Stack Moisture (%V)
Mole Fraction Dry Stack Gas
Dry Molecular Weight
Wet Molecular Weight
Stack Gas Velocity (fpm)
Stack Gas Velocity (mpm)
Volumetric Flow Rate (acfm)
Volumetric Flow Rate (acmm)
Volumetric Flow Rate (dscfm)
Volumetric Flow Rate (dscmm)
3ercent Isokinetic
Percent Excess Air
Concentration (g/dscm)
Concentration (kg/hr)
Concentration (ppmv)
Emissions (Ib/hr)
240.0
29.51
29.10
-5.60
198.00
8190.00
67.276
1.68
96.88
96.60
3.3
18.8
88.0
0.9840
0.103
0.84
0.259
62.045
1.757
6.84
0.932
32.07
31.11
6181.78
1884.21
351588.97
9957.00
255583.34
7238.12
99.42
416.70
0.00
0.00
0.00
0.00
-------
Facility:
Date:
Location:
Run Number:
Sample Type:
LTV East Chicago
6/25/97
Outlet
1
Multi metals
Total Sampling Time (min)
Corrected Barometric Pressure (in Hg)
Absolute Stack Pressure (in H2O)
Stack Static Pressure (in H2O)
Average Stack Temperature (°F)
Stack Area (sq in)
Actual Meter Volume (cu ft)
Average Meter Pressure (in H2O)
Average Meter Temperature (°F)
Moisture Collected (g)
Carbon Dioxide Concentration (%V)
Oxygen Concentration (%V)
Nitrogen Concentration (%V)
Dry Gas Meter Factor
Nozzle Diameter (in)
Pitot Constant
Average Sampling Rate (dscfm)
Standard Metered Volume (dscf)
Standard Metered Volume (dscm)
Stack Moisture (%V)
Mole Fraction Dry Stack Gas
Dry Molecular Weight
Wet Molecular Weight
Stack Gas Velocity (fpm)
Stack Gas Velocity (mpm)
Volumetric Flow Rate (acfm)
Volumetric Flow Rate (acmm)
Volumetric Flow Rate (dscfm)
Volumetric Flow Rate (dscmm)
Percent Isokinetic
Percent Excess Air
Concentration (g/dscm)
Concentration (kg/hr)
Concentration (ppmv)
Emissions (Ib/hr)
240.0
29.18
29.31
1.80
117.50
16286.02
166.707
0.83
92.17
404.40
3.5
17.5
79.0
0.9840
0.217
0.84
0.640
153.538
4.348
11.05
0.890
29.26
28.02
3013.70
918.58
340841.62
9652.63
271558.40
7690.53
103.74
519.01
0.00
0.00
0.00
0.00
-------
Facility:
Date:
Location:
Run Number:
Sample Type:
LTV East Chicago
6/26/97
Outlet
2
Multi metals
Total Sampling Time (min)
Corrected Barometric Pressure (in Hg)
Absolute Stack Pressure (in H2O)
Stack Static Pressure (in H2O)
Average Stack Temperature (°F)
Stack Area (sq in)
Actual Meter Volume (cu ft)
Average Meter Pressure (in H2O)
Average Meter Temperature (°F)
Moisture Collected (g)
Carbon Dioxide Concentration (%V)
Oxygen Concentration (%V)
Nitrogen Concentration (%V)
Dry Gas Meter Factor
Nozzle Diameter (in)
Pitot Constant
Average Sampling Rate (dscfm)
Standard Metered Volume (dscf)
Standard Metered Volume (dscm)
Stack Moisture (%V)
Mole Fraction Dry Stack Gas
Dry Molecular Weight.
Wet Molecular Weight
Stack Gas Velocity (fpm)
Stack Gas Velocity (mpm)
Volumetric Flow Rate (acfm)
Volumetric Flow Rate (acmm)
Volumetric Flow Rate (dscfm)
Volumetric Flow Rate (dscmm)
Percent Isokinetic
Percent Excess Air
Concentration (g/dscm)
Concentration (kg/hr)
Concentration (ppmv)
Emissions (Ib/hr)
240.0
29.35
29.36
0.18
117.83
16286.02
157.579
0.83
91.94
390.00
3.8
17.4
78.9
0.9840
0.217
0.84
0.608
146.035
4.136
11.18
0.888
29.30
28.03
2984.84
909.78
337576.99
9560.18
268854.67
7613.96
99.66
506.97
0.00
0.00
0.00
0.00
-------
Facility:
Date:
Location:
Run Number:
Sample Type:
LTV East Chicago
6/27/97
Outlet
3
Multi metals
Total Sampling Time (min)
Corrected Barometric Pressure (in Hg)
Absolute Stack Pressure (in H2O)
Stack Static Pressure (in H2O)
Average Stack Temperature (°F)
Stack Area (sq in)
Actual Meter Volume (cu ft)
Average Meter Pressure (in H2O)
Average Meter Temperature (°F)
Moisture Collected (g)
Carbon Dioxide Concentration (%V)
Oxygen Concentration (%V)
Nitrogen Concentration (%V)
Dry Gas Meter Factor
Nozzle Diameter (in)
Pitot Constant
Average Sampling Rate (dscfm)
Standard Metered Volume (dscf)
Standard Metered Volume (dscm)
Stack Moisture (%V)
Mole Fraction Dry Stack Gas
Dry Molecular Weight
Wet Molecular Weight
Stack Gas Velocity (fpm)
Stack Gas Velocity (mpm)
Volumetric Flow Rate (acfm)
Volumetric Flow Rate (acmm)
Volumetric Flow Rate (dscfm)
Volumetric Flow Rate (dscmm)
Percent Isokinetic
Percent Excess Air
Concentration (g/dscm)
Concentration (kg/hr)
Concentration (ppmv)
Emissions (Ib/hr)
240.0
29.40
29.41
0.18
116.46
16286.02
160.530
0.83
100.27
369.60
3.3
18.8
88.0
0.9840
0.217
0.84
0.612
-146.795
4.157
10.61
0.894
32.07
30.58
2865.84
873.51
324119.17
9179.06
260862.30
7387.62
103.25
416.70
0.00
0.00
0.00
0.00
-------
Facility:
Date:
Location:
Run Number:
Samole Tvoe:
LTV East Chicago
6/25/97
Outlet
1
Dioxin
Total Sampling Time (min)
Corrected Barometric Pressure (in Hg)
Absolute Stack Pressure (in H2O)
Stack Static Pressure (in H2O)
Average Stack Temperature (°F)
Stack Area (sq in)
Actual Meter Volume (cu ft)
Average Meter Pressure (in H2O)
Average Meter Temperature (°F)
Moisture Collected (g)
Carbon Dioxide Concentration (%V)
Oxygen Concentration (%V)
Nitrogen Concentration (%V)
Dry Gas Meter Factor
Nozzle Diameter (in)
Pitot Constant
Average Sampling Rate (dscfm)
Standard Metered Volume (dscf)
Standard Metered Volume (dscm)
Stack Moisture (%V)
Mole Fraction Dry Stack Gas
Dry Molecular Weight
Wet Molecular Weight
Stack Gas Velocity (fpm)
Stack Gas Velocity (mpm)
Volumetric Flow Rate (acfm)
Volumetric Flow Rate (acmm)
Volumetric Flow Rate (dscfm)
Volumetric Flow Rate (dscmm)
Percent Isokinetic
Percent Excess Air
Concentration (g/dscm)
Concentration (kg/hr)
Concentration (ppmv)
Emissions (lb/hr)_
240.0
29.18
29.31
1.80
117.46
16286.02
160.748
0.81
93.92
388.80
3.5
17.5
79.0
0.9960
0.217
0.84
0.622
149.293
4.228
10.94
0.891
29.26
28.03
2908.67
886.56
328962.48
9316.22
262438.55
7432.26
104.38
519.01
0.00
0.00
0.00
0.00
-------
Facility:
Date:
Location:
Run Number:
Sample Type:
LTV East Chicago
6/26/97
Outlet
2
Dioxin
Total Sampling Time (min)
Corrected Barometric Pressure (in Hg)
Absolute Stack Pressure (in H2O)
Stack Static Pressure (in H2O)
Average Stack Temperature (°F)
Stack Area (sq in)
Actual Meter Volume (cu ft)
Average Meter Pressure (in H2O)
Average Meter Temperature (°F)
Moisture Collected (g)
Carbon Dioxide Concentration (%V)
Oxygen Concentration (%V)
Nitrogen Concentration (%V)
Dry Gas Meter Factor
Nozzle Diameter (in)
Pitot Constant
Average Sampling Rate (dscfm)
Standard Metered Volume (dscf)
Standard Metered Volume (dscm)
Stack Moisture (%V)
Mole Fraction Dry Stack Gas
Dry Molecular Weight
Wet Molecular Weight
Stack Gas Velocity (fpm)
Stack Gas Velocity (mpm)
Volumetric Flow Rate (acfm)
Volumetric Flow Rate (acmm)
Volumetric Flow Rate (dscfm)
Volumetric Flow Rate (dscmm)
Percent Isokinetic
Percent Excess Air
Concentration (g/dscm)
Concentration (kg/hr)
Concentration (ppmv)
Emissions (Ib/hr)
240.0
29.35
29.36
0.18
117.33
16286.02
158.400
0.81
88.17
394.70
3.5
17.5
79.0
0.9960
0.217
0.84
0.623
149.562
4.236
11.07
0.889
29.26
28.01
2932.41
893.80
331647.76
9392.26
264711.06
7496.62
103.67
519.01
0.00
0.00
0.00
0.00
-------
TECHNICAL REPORT DATA
(Please read Instructions on reverse before completing)
1. REPORT NO. 2.
EPA- 454/R-99-042c
4. TITLE AND SUBTITLE
Integrated Iron and Steel Industry Final Report Manual Testing
Volume HI of III
LTV Steel Company Indiana Harbor Works East Chicago, Illinois
7. AUTHOR(S)
EMAD
9. PERFORMING ORGANIZATION NAME AND ADDRESS
U.S. Environmental Protection Agency
Office of Air Quality Planning and Standards
Research Triangle Park, NC 27711
12 SPONSORING AGENCY NAME AND ADDRESS
Director
Office of Air Quality Planning and Standards
Office of Air and Radiation
U.S. Environmental Protection Agency
Research Triangle Park, NC 27711
3. RECIPIENT'S ACCESSION NO.
5. REPORT DATE
August 1999
6. PERFORMING ORGANIZATION CODE
8. PERFORMING ORGANIZATION REPORT NO.
10. PROGRAM ELEMENT NO.
11. CONTRACT/GRANT NO.
68-D7-0068
13. TYPE OF REPORT AND PERIOD COVERED
Final
14. SPONSORING AGENCY CODE
EPA/200/04
15. SUPPLEMENTARY NOTES
16. ABSTRACT
Integrated iron and steel manufacturing is among the categories of major sources for
which national emission standards for hazardous air pollutants (NESHAPS) are to be issued by
November 2000 pursuant to Section 112 of the Clean Air Act. The integrated iron and steel
manufacturing category includes mills that produce steel from iron ore. Key processes and unit
operations include sinter production, iron production, steel making, continuous casting, and the
preparation of semi-finished and finished products. Source tests are required to quantify and
hazardous air pollutant (HAP) emissions, and the performance of a sintering plant equipped with
characterize the paniculate matter (PM), a venturi scrubber.
17
KEY WORDS AND DOCUMENT ANALYSIS
a DESCRIPTORS
Particulate Matter, Dioxin/Furan, PAH, Metals
18 DISTRIBUTION STATEMENT
Release Unlimited
b. IDENTIFIERS/OPEN ENDED TERMS
19. SECURITY CLASS (Report)
Unclassified
20 SECURITY CLASS (Page)
Unclassified
c. COSATI Field/Group
21. NO. OF PAGES
282
22. PRICE
'.PA Form 2220-1 (Rev. 4-77) PREVIOUS EDITION IS OBSOLETE
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