-------
Run No.
Date
Sampling Location Unit 2& Baohouse Outlet Duct
• Z.-7-
Project No. 104951.1.016.05.01
Operator
page.
of -2-
Sampling Data for Method 17 Train A No. M17-A
Traverse
Point
Sampling
Time,
min.
Clock
Time
(24-Hr)
Dry Gas Meter Reading
(Vm), ft3
Initial
Desired
Actual
Velocity
Head
(Ap),
in. H20
Orifice Pressure
Differential
(AH),
in. H2O
Desired
Actual
Stack
Temp.
Dry Gas Meter
Temperature
Inlet
Outlet
Pump
Vacuum,
in. Hg
Silica Gel
Impinger
Outlet
Temp.,
°F
C'f
2.3
2..I
-Zfl
7$-
^_
clef
ffff.ff
Ag-
rt.'TZ-
0.72-
J&L
$/*•#
a. 01
&2#ftf
2.)
2L
s*y
£2_
9j_
T.
2,7
z-f/
mji
2~£_
2.6!
ZL.
£2-
2E
XL
JJ&-
off*
fffrzr
2.V
II
rv
fo'l
ffgWJ-
^^_
-2.2,
-LL
ffl. 7a
/•la-
J&L-
totf
6?J-
•2-24
&=_
22-
/*>
roll
7
Olio
_fr^_
72_
^L
?*-
£L
1=5-
2*
80
<&_
2.0
J&-
/3
J&-
£L
5=2-
e>'
-------
40 CFR 60, APPENDIX A, METHOD 3B
INTEGRATED GAS SAMPLING DATA
Run No. 2-
Date g-27-f?
Client/Source U.S. EPA EMC / Coaentrix
Project No. 104951.1.016.05.01
Sample Type (Multi-Point, Single-Point)
Flow Control Device (Valve, Critical Orifice)
Method 5 Meter Box No.
MSB Pump Type Diaphram
MSB Pump No. n}"^
Sampling Location Unit 2A Baahouse Outlet Duct
Operator <^
Bag Type Mvlar
Method SB Train No. _
MSB Flow Meter Type
MSB Flow Meter No.
Sample No.
NA
NA
Rotameter
Desired Sampling Rate
Leak Check Before Sampling.
Total Sampling Time
cc/min
Flow Rate, cc/min: Average
Estimated Total Sample Volume
&_ After Sampling
min Average Flow Meter Reading
Highest
Lowest
liters
Time
(24-Hr)
Flow
Meter
Reading
Start
Purge
Start
Sampling
Stop
Sampling
Sampling
Remarks and Notes
otfi,
-b-0
01 if
1.'
1.'
&&
M3BSAMP.WPD June 18. 1998
10
RCA#1 APPENDIX C
-------
40 CFR 60, APPENDIX A, METHOD 3B, GAS ANALYSIS BY ORSAT
Run No.
Date
o
Project No. 104951.1.016.05.01 Sample No. NA - Train A
Sampling Location Unit 2A Baghouse Outlet Duct
Analysis Start Time
Sample Type (Bag, Grub)
Analyst ^
Bag
Orsat Leak Check Before Analysis:
Burrete __yv^L_ Change in 4 Minutes
Pipettes /V2> Change in 4 Minutes
Orsat Leak Check After Analysis:
Burrete /rt> Change in 4 Minutes
Pipettes Sr& Change in 4 Minutes
Analysis
Gas
C02
O2 (Net is actual reading
minus actual CO2 reading)
CO (Net is actual reading
minus actual 02 reading)
1
Actual
Reading
1 S&sV
2 ;£'•&
3
1 jty'Z--
2 x/2Z-
3
1
2
3
Net
Value
'
^
2
Actual
Reading
1 /S.O
2 J£~-V
3
1 )$>'2^
2 )9,'2^
3
1
2
3
Net
Value
J&-V
y,:2-
3
Actual
Reading
1 /*T't>
2 y^c-
3
1 W*-
2 y^^2-
3
1
2
3
Net
Value
X3'^
V-22-
Average
Net
Value
(% v/v)
^ '
V,Z_
Acceptance Criteria per Method 3B
C02 >4% 0.3% v/v
<4% 0.2% v/v
02 >15% 0.2% v/v
<15% 0.3% v/v
CO 0.3% v/v
Remarks and Notes:
M3BANAL.WPD May 28, 1999
-------
40 CFR 60, APPENDIX A, METHOD 17 - PARTICULATE MATTER TRAIN (M17)
FIELD LABORATORY TRAIN SET-UP DATA FOR TWO TRAINS
MRI Project No. 104951.1.016.05.01
Client/Source: U.S. EPA OAQPS EMAD EMC / Cogentrix Unit 2A
Source Location: Rocky Mount, North Carolina
Sampling Location: Baghouse (Fabric Filter) Outlet Duct
Run No. j3 Sampling Train A No. S&?/•?-
Sampling Train B No.
Set-up person(s): <->••
Impinger Box A No.,
Impinger Box B No. _
Date:
Transfer to Sampler:
Relinquished By el,
TRAIN COMPONENT
Received By.
REAGENT
. <£o'/Ao
Date/Time
LOADING DATA
TRAIN A
TRAIN B
Sampling Nozzle (Quartz)*
Filter Assembly and Holder*
Filter Type: Whatman 934-AH
Probe (316 SS)
Sample Transfer/Vacuum Line
Male 1st Impinger Inlet Blank-Off
Nozzle I.D. No.
Fitter Assembly No.
Filter Holder No.
Initial Weights (grams)
1st Impinger (Mod-GBS) 100-200 mLs ASTM Type I Water
U-Connector (A)
2nd Impinger (GBS) 100-200 mLs ASTM Type I Water
U-Connector (B)
3rd Impinger (Mod-GBS) Empty
U-Connector (C)
4th Impinger (Mod-GBS) "200 g indicating silica gel
U-Connector (D)
5th Impinger (Mod-GBS) » "
Impinger Outlet Connector
Connector I.D. No.
Before and after sampling: Nozzle inlet opening and filter assembly holder outlet opening covered with Teflon® tape, and
entire filter assembly holder with filter assembly and nozzle wrapped in aluminum foil and placed in Ziploc® bag. 1 st impinger
inlet sealed with glass blank-off.
Comments:
Ml7DSUP.WPD May 13, 1999 (rev. M17DSUP2.WPD July 29, 1999)
12
RCA#1 APPENDIX C
-------
40 CFR 60, APPENDIX A, METHOD 17 - PARTICULATE MATTER TRAIN (M17)
FIELD LABORATORY SAMPLE RECOVERY DATA FOR TWO TRAINS
MRI Project No. 104951.1.016.05.01
Client/Source: U.S. EPA OAQPS EMAD EMC / Cogentrix Unit 2A
Source Location: Rocky Mount, North Carolina
Sampling Location: Baghouse (Fabric Filter) Outlet Duct
Run No.
Sampling Train A No.
Sampling Train B No. J&s"?-
Impinger Box A No.
Impinger Box B No..
Transfer for Recovery:
Relinquished By &>
Received By
Date/Time
Sample recovery person(s):
Weights below are in grams.
Date:
BACK HALF RECOVERIES
TRAIN A
1st
873,*
Impinger:
Final Wt.
Initial Wt.
Net Wt.
Total Condensate Collected:
Description and/or color:
2nd
3rd
4th & 5th
1st
7.-}
% Blue
TRAIN B
2nd
3rd
4th & 5th
ffD.te
% Blue
FRONT HALF RECOVERIES
TRAIN A
FILTER ASSEMBLY:
Sample Number: .3102
PM Description/color: £>/•&&*
TRAIN RINSES:
Sample Number: ^2101
Components Rinsed*: nozzle, filter holder front
TRAIN B
104
103
* Acetone rinses with brushing 3 times or more until perceivably clean.
COMMENTS: Acetone rinses are transferred directly to tared Teflon® beaker liners for analysis.
M17DRCV.WPD May 13. 1999 (rev. M17DRCV2.WPD July 29, 1999)
13
RCA#1 APPENDIX C
-------
FIELD SAMPLING DATA FOR METHOD 17 TRAINS
s
Run No.
Date
- 1f
Project No. 104951.1.016.05.01
Client U.S. EPA EMC
Source Coaentrix Unit 2A
Sampling Location
h
Operator __M^iit»
Baahouse Oullel
Record dala every
Baromeler No.
mmules
Baromelric Pressure
Elevalion lo Meier Boxes _
/£,
Meier Box Pbar
Elevalion lo Sampling Loc.
Sampling Localion P,
Static Pressure
in Hg
34 ft
in Hg
34 ft
Train A No. M17-A
Probe No. A Lenath: 10 ft
Nozzle No./*//?-? Tio Dia. ^'/f£ in
Pilot Tube No. A Cp 0.84
Stack Thermocouole No. lljff'Ar
Filter Holder No. 5"
Filter Assembly No. Ir'*")
Impinaer Box No. T* V
Umbilical/lmpinqer Hookup it ff /
Umbilical No. (JL^'V
Meter Box No. 'lJ~l&
DGM Correction (Y) l,°W
Orifice Meter AH@ IrTftls
Train B No. M17-B
Probe No. B Length: 1 0 ft
Nozzle No. M/7'l\ Tip Dia. tf. I?L in
Pitol Tube No. B CD 0.84
Slack Thermocouole No. ^/ $& F)
Filter Holder No. t.
Filter Assemblv No. f~6
Impinaer Box No. O ~l
Umbilical/lmpinqer Hookup i£n 2-~
Umbilical No. U^O'l
Meter Box No. tJf\\
DGM Correclion (Y) //^£2
Orifice Meter AH@ l-fol
page 1 of
Traverse Point Layout
Assumed Moisture
Assumed %CO, / V'
%O,
Time (24 Hr)
Pass or Fail
/
Train A Pilot Tube Pressure Measuremenl System Leak Checks
Initial
nv*
Final
t'Hl
/1004
Initial
Final
Initial
Final
Initial
Final
Initial
Final
Train B Pitol Tube Pressure Measurement System Leak Checks
Initial
«fo
Final
/i • i+*
Initial
Final
Initial
Final
Initial
Final
Initial
Final
Train A Sampling System Leak Cnecks
Time (24 Hr)
Vacuum, in Hg
Leak Rate, cfm
Initial
11^
(<5
•00ft
Final Meter Volume
Initial Meter Volume
Leak Check Volume
Final
rt^
(0
,00^
Initial
Final
Initial
Final
Initial
Final
Initial
Final
O
Train B Sampling Syslem Leak Checks
Time (24 Hr)
Vacuum, in Hg
Leak Rate, cfm
Inilial
U^
l<»
.onis
Final Meier Volume
Inilial Meier Volume
Non-sample Volume
Final
^
iG,
-------
Run No. -s
Date
Sampling Location Unit 2A Baohouse Outlet Duct
Project No. 104951.1.016.05.01 Operator.
page "2- of 2.
Sampling Data for Method 17 Train A No. M17-A
Traverse
Point
Sampling
Time,
Clock
Time
(24-Hr)
Dry Gas Meter Reading
(VJ, ft3
Initial
Desired Actual
Velocity
Head
(Ap),
in. H2O
Orifice Pressure
Differential
(AH),
Desired Actual
Stack
Temp.
(ts),
°F
Dry Gas Meter
Temperature
Inlet
Outlet
Pump
Vacuum,
in. Hg
Silica Gel
Impinger
Outlet
Temp.,
°F
a?
f
JZ_
J^_
9*
891.*#,
a.Ll,
0.03
fs-
(2.16
SX6.25
-&L
£3-
•z-K
/?$
8"?
?7
0.08-
9*?
£•"?
"-7
z-7
97
9
/,*>
/Z-'/f
/*~f
{!&_
•Z..-7
9J-
~&
^£-
7-91-
It
4L-I
81
7-
/'•&
o.-tf
£S&-
9^-
vL
(•LIZ.
Z-L2-
SiL
us
t.<9
$*_
-i-
~T
t£2£_
ff.fO
a. to
3L
52-
mw
yz-
/#<$
72.
, 7?
2.-it
2^L
J&$-
9£_
$2^-
hi
-Z.SJ
73L
J3L
12,
ISL.
~W-
1
55
&&-
2. -7
S3-
zs
It.
I.T-f
/oc
i£L
^OL_
'ffft.
Si-
100
tfl.lr.00
0-2,1
Remarks and Notes:
M17DPG2.WPD July 2, 1999
RCA#1 APPENDIX C
15
-------
40 CFR 60, APPENDIX A, METHOD 3B
INTEGRATED GAS SAMPLING DATA
Run No.
Date
Project No. 104951.1.016.05.01
Sample Type (Multi-Point, Single-Point)
Flow Control Device (Valve, Critical Orifice)
Method 5 Meter Box No. /[)-/ After Sampling
min Average Flow Meter Reading
f± Highest.
Lowest
liters
Time
(24-Hr)
Flow
Meter
Reading
Start
Purge
Start
Sampling
Stop
Sampling
Sampling
Remarks and Notes
//vy
3.0
/-Z9?
10
IS
ftt-y
M3BSAMP.WPD June 18. 1998
16
RCA#1 APPENDIX C
-------
40 CFR 60, APPENDIX A, METHOD 3B, GAS ANALYSIS BY ORSAT
Run No.
Date
1
o
Project No. 104951.1.016.05.01 Sample No. NA - Train A
Sampling Location Unit 2A Baqhouse Outlet Duct
Analysis Start Time
Sample Type (Bag, Grab)
Analyst J/
Bag
Orsat Leak Check Before Analysis:
Burrete /^b Change in 4 Minutes
Pipettes /r£> Change in 4 Minutes
Orsat Leak Check After Analysis:
Burrete Sl^D Change in 4 Minutes
Pipettes X^b Change in 4 Minutes
Analysis
Gas
C02
O2 (Net is actual reading
minus actual CO2 reading)
CO (Net is actual reading
minus actual 02 reading)
1
Actual
Reading
1 X^7>
2 S&.0
3
1 y>£Z-
2 ;9/2-~
3
1
2
3
Net
Value
A£' ®
y-2-
2
Actual
Reading
1 ;&D
2 jjT,o
3
1 ./?,£-
2 /9,'i,
3
1
2
3
Net
Value
J£~.O
tJ-.Z-
3
Actual
Reading
1 ;gr.o
2 J&O
3
1 /^Z,
2 x^,2-
3
1
2
3
Net
Value
/&&
4-1*2
Average
Net
Value
(% v/v)
S&P
^4^
Acceptance Criteria per Method 3B
C02 >4% 0.3% v/v O2 >15% 0.2% v/v CO
<4% 0.2% v/v <15% 0.3% v/v
0.3% v/v
Remarks and Notes:
M3BANAL.WPD Mav 28, 1999
-------
40 CFR 60, APPENDIX A, METHOD 17 - PARTICULATE MATTER TRAIN (M17)
FIELD LABORATORY TRAIN SET-UP DATA FOR TWO TRAINS
MRI Project No. 104951.1.016.05.01
Client/Source: U.S. EPA OAQPS EMAD EMC / Cogentrix Unit 2A
Source Location: Rocky Mount, North Carolina
Sampling Location: Baghouse (Fabric Filter) Outlet Duct
Run No. i Sampling Train A No.
Sampling Train B No.
Set-up person(s): C/
Transfer to Sampler:
Relinquished By J, £10^^73*7 Received By
TRAIN COMPONENT
REAGENT
Impinger Box A No.
Impinger Box B No. .
Date:
Date/Time
LOADING DATA
TRAIN A
Sampling Nozzle (Quartz)*
Filter Assembly and Holder*
Filter Type: Whatman 934-AH
Probe (316SS)
Sample Transfer/Vacuum Line
Male 1st Impinger Inlet Blank-Off
TRAIN B
Nozzle I.D. No.
Fitter Assembly No.
Filter Holder No.
1st Impinger (Mod-GBS) 100-200 mLs ASTM Type I Water
U-Connector (A)
2nd Impinger (GBS) 100-200 mLs ASTM Type I Water
U-Connector (B)
3rd Impinger (Mod-GBS) Empty
U-Connector (C)
4th Impinger (Mod-GBS) "200 g indicating silica gel
U-Connector (D)
5th Impinger (Mod-GBS) {> js
Impinger Outlet Connector
Connector I.D. No.
t*
Initial Weights (grams)
* Before and after sampling: Nozzle inlet opening and filter assembly holder outlet opening covered with Teflon® tape, and
entire filter assembly holder with filter assembly and nozzle wrapped in aluminum foil and placed in Ziploc® bag. 1st impinger
inlet sealed with glass blank-off.
Comments:
M17DSUP.WPD Mav 13. 1999 (rev. M17DSUP2.WPD July 29. 1999)
18
RCA#1 APPENDIX C
-------
40 CFR 60, APPENDIX A, METHOD 17 - PARTICULATE MATTER TRAIN (M17)
FIELD LABORATORY SAMPLE RECOVERY DATA FOR TWO TRAINS
MRI Project No. 104951.1.016.05.01
Client/Source: U.S. EPA OAQPS EMAD EMC / Cogentrix Unit 2A
Source Location: Rocky Mount, North Carolina
Sampling Location: Baghouse (Fabric Filter) Outlet Duct
Run No. 3
Sampling Train A No.
Sampling Train B No.
Transfer for Recovery:
Relinquished By £>.
Received By «•*,
Impinger Box A No.
Impinger Box B No.
Date/Time
Sample recovery person(s):
Weights below are in grams.
t), S
Date:
BACK HALF RECOVERIES
TRAIN A
TRAIN B
1st
Impinger:
Final Wt.
Initial Wt.
Net Wt.
Total Condensate Collected:
Description and/or color:
2nd
3rd
4th & 5th
1st
2nd
3rd
V7JV
4th & 5th
ft*
/>*
9M
% Blue
FRONT HALF RECOVERIES
% Blue
TRAIN A
TRAIN B
^104
FILTER ASSEMBLY:
Sample Number: JT102
PM Description/color: _
TRAIN RINSES:
Sample Number:
Components Rinsed*: nozzle, filter holder front
* Acetone rinses with brushing 3 times or more until perceivably clean.
COMMENTS: Acetone rinses are transferred directly to tared Teflon® beaker liners for analysis.
M17DRCV.WPD Mav 13, 1999 (rev. M17DRCV2.WPD July 29. 19991
RCA#1 APPENDIX C
19
-------
CO
FIELD SAMPLING DATA FOR METHOD 17 TRAINS
page 1 of
Run No. V
Date
t'Zl-'ff
Project No. 104951.1.016.05.01
Client U.S. EPA EMC
Source Coqentrix Unit 2A
Sampling Loca
Operator fit
Record data e
Barometer No
Barometric Pre
Elevation to IV
Meter Box Pba,
Elevation to S
Sampling LOCE
Static Pressur
Time (24 Hr)
Pass or Fail
tion, Bacihouse Outlet
r^— '
/ery v minutes
assure "K
eter Boxes
/I
ampling Loc
tion Ptl,
sj£f-#
Train A
Initial Fir
Lt^l/ ^l
ja
'/
I.'?? in
34
fr1
;
6-2-
Hookup
> / ^C^7^~
A)-l\
tiff}.
1
Z-
DGM Correction (Y) /.0i3
Orifice Meter AH@
3/o Assumed %CO2 /'
Pitot Tube Pressure Measurement System Leak Checks
lal Initial
14
Final
Initial
Final
Initial
Final
Initial
Final
f.W
t*> %
0, fa
•>
<
//
\l
Y
^
\
^
^h
^
\
^
^
/
1^ j i j L_/ T— i L-/
A ft
-------
Run No.
Date &-'<
Sampling Location Unit 2A Baahouse Outlet Duct
Project No. 104951.1.016.05.01
Operator
page.
of
Sampling Data for Method 17 Train A No. M17-A
Traverse
Point
Sampling
Time,
min.
Clock
Time
(24-Hr)
~ML
Dry Gas Meter Reading
(VJ, ft3
Initial
Desired
Actual
Velocity
Head
(Ap),
in. H20
Orifice Pressure
Differential
(AH),
Desired
Actual
Stack
Temp.
ft.),
°F
Dry Gas Meter
Temperature
(tj,
°F
Inlet Outlet
Pump
Vacuum,
in. Hg
Silica Gel
Impinger
Outlet
Temp.,
c-f
Z,^
2*3_
•7-f
/L^_
^_
ti-
L*t-
M-
ll
•7
o.0(.
•2..1
-¥-
*.!(,
2.2-
tec,
G6f.fr
41
7T
j&f_
JteL
?£_
^.^
a,19
kf
£2^
j^=-
,2^_
^Z^
/^//
^
/a
/Of>
s*
•2.J9
7
f^-
7.^7
-^_
/Z.
1&.79
5-^
z/
fit*
^^9
2-/
Z2_
Aff
^=L
YS
0.X f
ff
j^5L
c-f
^... *f,
*ll**l
/#*
/3_
^^_
Z^.
^-
*79
0.0L
z./g
g-/
/J&L
I/
^_
^^7
v^-
•2 ^7
59
V
s?
2.3
f-1
.
/v
l*L
/£>
(4C_
t fOo
Q.&
4%_
Remarks and Notes:
M17DPG2.WPD July 2. 1999
RCA#l APPENDIX C
21
-------
40 CFR 60, APPENDIX A, METHOD 3B
INTEGRATED GAS SAMPLING DATA
Run No..
Date
Client/Source U.S. EPA EMC / Coaentrix
Project No. 104951.1.016.05.01 _
Sample Type (Multi-Point, Single-Point)
Flow Control Device (Valve, Critical Orifice)
Method 5 Meter Box No. ^J 1C _
MSB Pump Type Diaphram _
MSB Pump No.
Sampling Location Unit 2A Baohouse Outlet Duct
Operator
Bag Type Mvlar
Method SB Train No. _
MSB Flow Meter Type.
MSB Flow Meter No.
Sample No.
NA
NA
Rotameter
Desired Sampling Rate
Leak Check Before Sampling
Total Sampling Time is
cc/min
Flow Rate, cc/min: Average
Estimated Total Sample Volume
<^ After Sampling
min Average Flow Meter Reading
Highest 3°°-
Lowest
liters
Time
(24-Hr)
Flow
Meter
Reading
Start
Purge
Start
Sampling
Stop
Sampling
Sampling
Remarks and Notes
(W*
I'll I
If
•3.*
& is
3,0
M3BSAMP.WPD June 18. 1998
u
22
RCA#1 APPENDIX C
-------
40 CFR 60, APPENDIX A, METHOD 3B, GAS ANALYSIS BY ORSAT
0
m
o
Run No.
Date
Project No. 104951.1.016.05.01 Sample No. NA - Train A
Sampling Location Unit 2A Baghouse Outlet Duct
Analysis Start Time
Sample Type (Bag, Grab)
Analyst Change in 4 Minutes
Pipettes A^> Change in 4 Minutes
Orsat Leak Check After Analysis:
Burrete Sfo Change in 4 Minutes
Pipettes
^•2.
Average
Net
Value
(% v/v)
J5~;}
^.*2—
Acceptance Criteria per Method 3B
C02 >4%0.3%v/v
<4% 0.2% v/v
02 ^15% 0.2% v/v
<15% 0.3% v/v
CO 0.3% v/v
Remarks and Notes:
ro
CO
M3BANAL.WPD May 28. 1999
-------
40 CFR 60, APPENDIX A, METHOD 17 - PARTICULATE MATTER TRAIN (M17)
FIELD LABORATORY TRAIN SET-UP DATA FOR TWO TRAINS
MRI Project No. 104951.1.016.05.01
Client/Source: U.S. EPA OAQPS EMAD EMC / Cogentrix Unit 2A
Source Location: Rocky Mount, North Carolina
Sampling Location: Baghouse (Fabric Filter) Outlet Duct
Run No. y Sampling Train A No.,
Sampling Train B No..
Set-up person(s): *)>
Transfer to Sampler: ^
Relinquished By eJj
Impinger Box A No.
Impinger Box B No.
Date:
Received By
Date/Time
TRAIN COMPONENT
REAGENT
LOADING DATA
TRAIN A
TRAIN B
Sampling Nozzle (Quartz)*
Filter Assembly and Holder*
Filter Type: Whatman 934-AH
Probe (316 SS)
Sample Transfer/Vacuum Line
Male 1st Impinger Inlet Blank-Off
Nozzle I.D. No.
Filter Assembly No.
Filter Holder No.
2
Initial Weights (grams)
1st Impinger (Mod-GBS) 100-200 mLs ASTM Type I Water
U-Connector (A)
2nd Impinger (GBS) 100-200 mLs ASTM Type I Water
U-Connector (B)
3rd Impinger (Mod-GBS) Empty
U-Connector (C)
4th Impinger (Mod-GBS) "200 g indicating silica gel
U-Connector (D)
5th Impinger (Mod-GBS) "
''
Impinger Outlet Connector
Connector I.D. No.
Before and after sampling: Nozzle inlet opening and filter assembly holder outlet opening covered with Teflon® tape, and
entire filter assembly holder with filter assembly and nozzle wrapped in aluminum foil and placed in Ziploc® bag. 1 st impinger
inlet sealed with glass blank-off.
Comments:
M17DSUP.WPD May 13. 1999 (rev. M17DSUP2.WPD July 29. 1999)
24
RCA#1 APPENDIX C
-------
40 CFR 60, APPENDIX A, METHOD 17 - PARTICULATE MATTER TRAIN (M17)
FIELD LABORATORY SAMPLE RECOVERY DATA FOR TWO TRAINS
MRI Project No. 104951.1.016.05.01
Client/Source: U.S. EPA OAQPS EMAD EMC / Cogentrix Unit 2A
Source Location: Rocky Mount, North Carolina
Sampling Location: Baghouse (Fabric Filter) Outlet Duct
Run No.
Sampling Train A No.
Sampling Train B No..
Transfer for Recovery:
Relinquished By £2 &f,f~Ti-r>
Received By (J.
Impinger Box A No.
Impinger Box B No..
Date/Time
Sample recovery person(s):
Weights below are in grams.
Date:
BACK HALF RECOVERIES
TRAIN A
1st
Impinger:
Final Wt.
Initial Wt.
Net Wt.
Total Condensate Collected:
Description and/or color:
2nd
3rd
4th & 5th
1 st
/7
% Blue
TRAIN B
2nd
3rd
4th & 5th
£>•(<>
&3P.3
% Blue
FRONT HALF RECOVERIES
TRAIN A
FILTER ASSEMBLY:
Sample Number: V102
PM Description/color: ^3/3cA-
TRAIN RINSES:
Sample Number: V101
Components Rinsed*: nozzle, filter holder front
TRAIN B
^104
V03
* Acetone rinses with brushing 3 times or more until perceivably clean.
COMMENTS: Acetone rinses are transferred directly to tared Teflon® beaker liners for analysis.
M17DRCV.WPD May 13, 1999 [rev. M17DRCV2.WPD July 29, 1999)
RCA#1 APPENDIX C
25
-------
ro
FIELD SAMPLING DATA FOR METHOD 17 TRAINS
page 1 of
•2-
Run No. ^ Date f'"2£'™
Project No. 104951.
Client U.S. EPA EMC
.016.05.01
Source Coaentrix Unit 2A
RCA#1 APPENDIX (
Sampling LOCE
Operator (as
Record data e
Barometer No
Barometric Pr«
Elevation to IV
Meter Box Pba,
Elevation to S
Sampling LOCE
Static Pressur
Time (24 Hr)
Pass or Fail
Time (24 Hr)
tion Baahouse Outlet
$-
i/erv
7 '
;ssure
7 minutes
1(0 '
2.T.86.
eter Boxes
ampling
tion Pba,
a t?-<>
CLtf'09
Loc.
13,%*>
in Hg
34 ft
in Hg
34 ft
in Hg
Train A No. M1
Probe No. A
Nozzle Nc
Pitot Tub
Stack Th
Filter Hol<
Filter Ass
Impinger
Umbilical
Umbilical
7-A
Lenqth:
B No. A
srmocouple No.
Jer No.
embly ^
Box No.
Jo.
Dia. d.
Cp
10 ft
#<5 in
0.84
1(7? A-
/
^"-^
A-l
'Impinger Hook
No. // 5°
JD UH-1
-Y
Meter Box No. ^^n^.&f^- /(/~(0
DGM Correction (Y) ftflf
Orifice Meter AH<5> /- £32---
t *r3>£>7 |n H2O Assumed
Train A Pitot
Initial
(TO
Final Ir
[cHH
J>03.f>
'
Initial
O'fal'
Moisture H'O
Train B No.
Probe No.
M17-B
B
Nozzle No. /Hf/-t
Pitot Tube \
Stack Therr
Filter Holde
Filter Assen
Impinger Be
Umbilical/lrr
Umbilical N
^Jo. B
nocoupl
r No.
nbly No.
x No.
ipinger I
0.
Meter Box No.
DGM Correction (Y)
Orifice Meter AH@
Lengl
Tip Dia
2 No. ^
2-
h: 1<
. 0.12*1
D ft
1 in
3p 0.84
'iff $
C-(o
$-/
Hookup
d/5£»'/
N-tl
f,c
Iftfi^
^J
l.lol
1
\
*sr
;i
YJ
5" l
1
5X
K. '
^
^
/
2 & c y ^
Traverse Point Layout
% Assumed %CO2 If* ' %O2 H.t-
Tube Pressure Measurement System Leak Checks
itial Final
Final
(OW
Initial
Final
Initial
Initial
Train
Final
Initial
Final
A Sampling System
Final
Initial
Train B Pitot Tube Pressure Measurement System Leak Checks
Initial
0836>
Leak
-------
Run No. -5"
Date
Sampling Location Unit 2A Baahouse Outlet Duct
Project No. 104951.1.016.05.01
Operator
9*
106
effr-
Sampling Data for Method 17 Train B No. M17-B
•2.0
•72_
"/•
•2.0
<*
71
.t,
,.2-f
go
•7
CtfH
f.Zb
^4-
J^L
&OL
is
,% 1
12.2, ?ft
2*1
/-t,
Si.
T2--7,
QJttf
JL
•7
i^_
So
Iff i
•18$
£L
J^.
'*
fO
-aJH-
.(L-IL
US-
Remarks and Notes:
M17DPG2.WPD July 2. 1999
76
RCA#1 APPENDIX C
27
-------
40 CFR 60, APPENDIX A, METHOD 3B
INTEGRATED GAS SAMPLING DATA
Run No. 5
Project No. 104951.1.016.05.01
Sample Type (Multi-Point, Single-Point)
Flow Control Device (Valve, Critical Orifice)
Method 5 Meter Box No.
MSB Pump Type Diaphram
MSB Pump No. /!/' 10
Client/Source U.S. EPA EMC / Coaentrix
Sampling Location Unit 2A Baahouse Outlet Duct
Operator
Bag Type Mvlar _
Method SB Train No._
MSB Flow Meter Type
MSB Flow Meter No.
Sample No.
NA
NA
Rotameter
Desired Sampling Rate 30°-
Leak Check Before Sampling £
Total Sampling Time
cc/min
Flow Rate, cc/min: Average
Estimated Total Sample Volume
'_ After Sampling
min Average Flow Meter Reading
Highest ~3
-------
40 CFR 60, APPENDIX A, METHOD 3B, GAS ANALYSIS BY ORSAT
I
o
Run No.
Date
Project No. 104951.1.016,05.01 Sample No. NA - Train A
Sampling Location Unit 2A Baghouse Outlet Duct
Analysis Start Time
Sample Type (Bag, Grab)
Analyst J'Si.
Bag
Orsat Leak Check Before Analysis:
Burrete S/v Change in 4 Minutes
Pipettes /Yo Change in 4 Minutes
Orsat Leak Check After Analysis:
Burrete /?b Change in 4 Minutes
Pipettes Sift Change in 4 Minutes
Analysis
Gas
C02
02 (Net is actual reading
minus actual CO2 reading)
CO (Net is actual reading
minus actual O2 reading)
1
Actual
Reading
1 s&t>
2 J&D
3
1 /9.Z-
2 /#2-
3
1
2
3
Net
Value
/^>.O
*j.2-
2
Actual
Reading
1 /*7P
2. _• ^%
J£tO
3
1 ;%2-
2 />2iZ-
3
1
2
3
Net
Value
Ag~,<2
y.tZ-
3
Actual
Reading
1 /3~^#
2 jg~.c>
3
1 ;9.?-
2 /i?,2_
3
1
2
3
Net
Value
J£>~,o
y^
Average
Net
Value
{% v/v)
J^a~.D
V.2-
Acceptance Criteria per Method 3B
C02 >4% 0.3% v/v
<4% 0.2% v/v
O2 >15% 0.2% v/v
<15% 0.3% v/v
CO 0.3% v/v
Remarks and Notes:
ro
M3BANAL.WPD May 28, 1999
-------
40 CFR 60, APPENDIX A, METHOD 17 - PARTICULATE MATTER TRAIN (M17)
FIELD LABORATORY TRAIN SET-UP DATA FOR TWO TRAINS
MRI Project No. 104951.1.016.05.01
Client/Source: U.S. EPA OAQPS EMAD EMC / Cogentrix Unit 2A
Source Location: Rocky Mount, North Carolina
Sampling Location: Bagnouse (Fabric Filter) Outlet Duct
Run No.
Set-up person(s): J.
Transfer to Sampler:
Relinquished By »J.
Sampling Train A No.
Sampling Train B No.
Impinger Box A No. _
Impinger Box B No. J&~ •
Date:
Received By &
Date/Time
TRAIN COMPONENT
REAGENT
Sampling Nozzle (Quartz)*
Filter Assembly and Holder*
Filter Type: Whatman 934-AH
Probe (316 SS)
Sample Transfer/Vacuum Line
Male 1st Impinger Inlet Blank-Off
LOADING DATA
TRAIN A
TRAIN B
Nozzle I.D. No.
Filter Assembly No.
Filter Holder No.
Initial Weights (grams)
1st Impinger (Mod-GBS) 100-200 mLs ASTM Type I Water
U-Connector (A)
2nd Impinger (GBS) 100-200 mLs ASTM Type I Water
U-Connector (B)
3rd Impinger (Mod-GBS) Empty
U-Connector (C)
4th Impinger (Mod-GBS) "200 g indicating silica gel
U-Connector (D)
5th Impinger (Mod-GBS) // "
Impinger Outlet Connector
Connector I.D. No.
* Before and after sampling: Nozzle inlet opening and filter assembly holder outlet opening covered with Teflon® tape, and
entire filter assembly holder with filter assembly and nozzle wrapped in aluminum foil and placed in Ziploc® bag. 1 st impinger
inlet sealed with glass blank-off.
Comments:
M17DSUP.WPD May 13, 1999 (rev. M17DSUP2.WPD July 29, 19991
30
RCA#1 APPENDIX C
-------
40 CFR 60, APPENDIX A, METHOD 17 - PARTICULATE MATTER TRAIN (M17)
FIELD LABORATORY SAMPLE RECOVERY DATA FOR TWO TRAINS
MRI Project No. 104951.1.016.05.01
Client/Source: U.S. EPA OAQPS EMAD EMC / Cogentrix Unit 2A
Source Location: Rocky Mount, North Carolina
Sampling Location: Baghouse (Fabric Filter) Outlet Duct
Run No.
Sampling Train A No.
Sampling Train B No..
Impinger Box A No.
Impinger Box B No..
Transfer for Recovery:
Relinquished By £?..
Received By.
Date/Time
Sample recovery person(s):
Weights below are in grams.
>J,i
Date: #£-3/--?5
BACK HALF RECOVERIES
TRAIN A
1st
Impinger:
Final Wt.
Initial Wt.
Net Wt.
Total Condensate Collected:
Description and/or color:
2nd
3rd
4th & 5th
7
1st
79S.*/
?3- ?£>*'»
% Blue
TRAIN B
2nd
3rd
4th & 5th
S&&.D
0,7
% Blue
FRONT HALF RECOVERtES
TRAIN A
FILTER ASSEMBLY:
Sample Number: ^102
PM Description/color: _
TRAIN RINSES:
Sample Number:
Components Rinsed*: nozzle, filter holder front
TRAIN B
* Acetone rinses with brushing 3 times or more until perceivably clean.
COMMENTS: Acetone rinses are transferred directly to tared Teflon® beaker liners for analysis.
M17DRCV.WPD May 13, 1999 (rev. M17DRCV2.WPD July 29, 19991
RCA#1 APPENDIX C
31
-------
CO
I
iS
n
FIELD SAMPLING DATA FOR METHOD 17 TRAINS
Run No. .
Date
Project No. 104951.1.016.05.01
Client U.S. EPA EMC
Source Cogentrix Unit 2A
Sampling Location
Operator
Baahouse Outlet
Record data every .
Barometer No.
minutes
Barometric Pressure
Elevation to Meter Boxes
Meter Box Pba, 2f
Elevation to Sampling Loc..
Sampling Location Pbar ^
Static Pressure
in Hg
34 ft
in Hg
34 ft
in Hg
-m ^^Q
Train A No. M17-A
Probe No. A Lenqth: 10 ft
Nozzle No. /Jf(-H2 Tip Dia. O.fti, in
Pitot Tube No. A CD 0.84
Stack Thermocouple No. ^l^ff ft
Filter Holder No. *?
Filter Assembly No. f"((
Impinaer Box No. /r2-"
Umbilical/lmpinger Hookup IA (r ^0
Umbilical No. /Jl^' t
Meter Box No. fj \a
DGM Correction (Y) {-Off
Orifice Meter AH@ /, # ^1^
Train B No. M17-B
Probe No. B Lenath: 1 0 ft
Nozzle No. f\ tf'M Tio Dia. • \8*f in
Pitot Tube No. B CD 0.84
Stack Thermocouple No. 111? *
Filter Holder No. ¥
Filter Assembly No. P-/Z-
Impinqer Box No. P ~2—
Umbilical/lmpinqer Hookup M-n 9/2--
Umbilical No. AJfy "/
Meter Box No. fi) ll
DGM Correction (Y) / . O-Z. *)
Orifice Meter AH@ (, 1& /
page 1 of
LJ l-Jf-3f LJ
fir ft C P £
Traverse Point Layout
Assumed Moisture
% Assumed %CO2
%O2 ¥
Time (24 Hr)
Pass or Fail
Time (24 Hr)
Vacuum, in Hg
Leak Rate, cfm
Train A Pitot Tube Pressure Measurement System Leak Checks
Initial
\v*
Final
/Wr
jOOA*
/
Initial
,<7
-------
Run No.
Date
Sampling Location Unit 2A Baahouse Outlet Duct
Project No. 104951.1.016.05.01
Operator.
page.
of
^
Sampling Data for Method 17 Train A No. M17-A
Sampling
Time,
Traverse
Point
Clock
Time
24-Hr)
1&L
Dry Gas Meter Reading
-7
W
r*
^
L
/'
19*
^22,
4K.^
/t-
its
(*-
A£
/if
0.20
60
/3/y
-UU
~w
2-0
701
±&L.
fey
/t—
f/8,fy
0,16
Ml
Sampling Data for Method 17 Train B No. M17-B
1-9H
(•*
3L
(3
-U2-
(81
*tt-
It
4^
•fr-
II
17_
0.93
¥7
10
lleZ
50
zy
ps±
2,3
1,1
.1
n
u±
a. 11
ffS
'
/
31
3£.
3L
^SL
1-2
J^SL
f^
(00
ZL
o-tf
1*1
(ft
So
c
1..-L.
4^L
T
72-
t-1-
U-
J3L
let.
76
LJff^-ZJ.
<>>&(,
725-
tol
jfe.
a.on
yy
t*
1..0
fro
1.2.1
lot
ffb
*ff7" ^7
0.10
o.1t>
53
Remarks and Notes:
M17DPG2.WPD July 2. 1999
76
RCA#1 APPENDIX C
33
-------
40 CFR 60, APPENDIX A, METHOD 3B
INTEGRATED GAS SAMPLING DATA
Run No.
Date
Client/Source U.S. EPA EMC / Cooentrix
Project No. 104951.1.016.05.01
Sample Type (Multi-Point, Single-Point)
Flow Control Device (Valve, Critical Orifice)
Method 5 Meter Box No.
MSB Pump Type Diaphram
MSB Pump No.
Sampling Location Unit 2A Baahouse Outlet Duct
Operator <5rr
-------
40 CFR 60, APPENDIX A, METHOD 3B, GAS ANALYSIS BY ORSAT
Run No.
Date
o
6
i
n
Project No. 104951.1.016.05.01 Sample No. NA - Train A
Sampling Location Unit 2A Baghouse Outlet Duct
Analysis Start Time
Sample Type (Bag, Grab)
Analyst t/
Bao
Orsat Leak Check Before Analysis:
Burrete /)/o Change in 4 Minutes
Pipettes A*v Change in 4 Minutes
Orsat Leak Check After Analysis:
Burrete /^P Change in 4 Minutes
Pipettes /fa Change in 4 Minutes
Analysis
Gas
C02
O2 (Net is actual reading
minus actual CO2 reading)
CO (Net is actual reading
minus actual 02 reading)
1
Actual
Reading
1 /&*
*} S^i* ^
3
1J & "7
' C?-U?
2 J£3
3
1
2
3
Net
Value
/45J2.
w
2
Actual
Reading
1 S&-2
2 J&,2
3
1 SfJ
2 X/J?
3
1
2
3
Net
Value
S£~.'2-
f.S
3
Actual
Reading
1 J&l*
2 /cSTTZ-
3
1 X/JJ
2 y/^
3
1
2
3
Net
Value
^^57 z^
4*-J
Average
Net
Value
(% v/v)
X^- 2—
4*'J
Acceptance Criteria per Method 3B
C02 >4%0.3%v/v O2 >15% 0.2% v/v CO
<4% 0.2% v/v <15% 0.3% v/v
0.3% v/v
Remarks and Notes:
co
en
M3BANAL.WPD May 28. 1999
-------
40 CFR 60, APPENDIX A, METHOD 17 - PARTICULATE MATTER TRAIN (M17)
FIELD LABORATORY TRAIN SET-UP DATA FOR TWO TRAINS
MRI Project No. 104951.1.016.05.01
Client/Source: U.S. EPA OAQPS EMAD EMC / Cogentrix Unit 2A
Source Location: Rocky Mount, North Carolina
Sampling Location: Baghouse (Fabric Filter) Outlet Duct
Run No.
Sampling Train A No.
Sampling Train B No. S*) ;•?-
Set-up person(s): J • £i.4
Transfer to Sampler:
Impinger Box A No.
Impinger Box B No..
Date:
Relinquished By J. S
Received By
Date/Time
TRAIN COMPONENT
REAGENT
LOADING DATA
TRAIN A
TRAIN B
Sampling Nozzle (Quartz)*
Filter Assembly and Holder*
Filter Type: Whatman 934-AH
Probe (316 SS)
Sample Transfer/Vacuum Line
Male 1st Impinger Inlet Blank-Off
Nozzle I.D. No.
Filter Assembly No.
Filter Holder No.
Initial Weights (grams)
1st Impinger (Mod-GBS) 100-200 mLs ASTM Type I Water
U-Connector (A)
2nd Impinger (GBS) 100-200 mLs ASTM Type I Water
U-Connector (B) sx
3rd Impinger (Mod-GBS) Empty
U-Connector (C)
4th Impinger (Mod-GBS) "200 g indicating silica gel
U-Connector (D)
5th Impinger (Mod-GBS) H f
>£9
Impinger Outlet Connector
Connector I.D. No.
Before and after sampling: Nozzle inlet opening and filter assembly holder outlet opening covered with Teflon® tape, and
entire filter assembly holder with filter assembly and nozzle wrapped in aluminum foil and placed in Ziploc® bag. 1 st impinger
inlet sealed with glass blank-off.
Comments:
M17DSUP.WPD May 13. 1999 Irev. M17DSUPZ.WPD July 29. 19991
36
RCA#1 APPENDIX C
-------
40 CFR 60, APPENDIX A, METHOD 17 - PARTICULATE MATTER TRAIN (M17)
FIELD LABORATORY SAMPLE RECOVERY DATA FOR TWO TRAINS
MRI Project No. 104951.1.016.05.01
Client/Source: U.S. EPA OAQPS EMAD EMC / Cogentrix Unit 2A
Source Location: Rocky Mount, North Carolina
Sampling Location: Baghouse (Fabric Filter) Outlet Duct
Run No. u?
Sampling Train A No. /%V7v9
Sampling Train B No.
Impinger Box. A No..
Impinger Box B No..
Transfer for Recovery:
Relinquished By 17-
Received By,
Date/Time
Sample recovery person(s):
Weights below are in grams.
Date:
BACK HALF RECOVERIES
TRAIN A
Impinger: 1st
Final Wt. £&, S
Initial Wt. &S&3
Net Wt.
2nd
3rd
4th & 5th
1st
. e
Z.V
Total Condensate Collected:
Description and/or color:
% Blue
TRAIN B
2nd
3rd
4th & 5th
% Blue
FRONT HALF RECOVERIES
TRAIN A
FILTER ASSEMBLY:
Sample Number: ^102
PM Description/color: b)-3-&k.
TRAIN RINSES:
Sample Number: ^ 101
Components Rinsed*: nozzle, filter holder front
TRAIN B
104
* Acetone rinses with brushing 3 times or more until perceivably clean.
COMMENTS: Acetone rinses are transferred directly to tared Teflon® beaker liners for analysis.
M17DRCV.WPD May 13. 1999 (rev. M17DRCV2.WPD July 29, 19991
RCA#1 APPENDIX C
37
-------
CO
oo
FIELD SAMPLING DATA FOR METHOD 17 TRAINS
Run No. *7 Date
Project No. 104951.1.016.05.01
Client U.S. EPA EMC
Source Coaentrix Unit 2A
Sampling Location
Operator _ t^r
Baohouse Outlet
Record data every
Barometer No.
minutes
Barometric Pressure
Elevation to Meter Boxes .
Meter Box Pba, li
in Hg
34 ft
Elevation to Sampling Loc.
Sampling Location Pba,
in Hg
34 — ft
in Hg
Train A No M1 7-A
Probe No. A Length: 1 0 ft
Nozzle No M\1~^ TJD Dia. 0'lff£ in
Pitnt Tube No. A Cf 0.84
Stark Thprmnrniiple No. y/xv" ^
Filter Holder No. ^~
Filter Assembly No. ^"/'
ImpinQff Box No. /? ~(
Umbiliral/lrnpinner Hookup pv t\ f
llmhiliral No &l*?&-tj
Mpfpr Rnx No. t*J /&
PGM rnrrer.tinn (Y) (, &(l
nrifire Meter AH© ('frlZ-
Train B No. M17-B
Probe No. B Length: 10 ft
Mn77li>No Mrt-tr Tip Dia. ir
Traverse Point Layout
% Assumed %CO2
%O2
Static Kressur
Time (24 Hr)
Pass or Fail
Train A Pitot Tube Pressure Measurement System Leak Checks
Initial
/^cJ^
Final
Urf'f
JD006
Initial
Final
Initial
Final
Initial
Final
Initial
Final
Train B Pitot Tube Pressure Measurement System Leak Checks
Initial
/$JV
Final
(ltf\
-J/XIA
Initial
Final
Initial
Final
Initial
Final
Initial
hmal
o
Train A Sampling System Leak Checks
Tin
te (24 Hr)
k Rate, cfm
— i^ltuii — I
/*/li
< fr " j(/c
,0o$
Final Meter Volume
Initial Meter Volume
Leak Check Volume
Final
\^
10
\ .<*[
Initial
Final
Initial
Final
Initial
Final
Initial
Final
Train B Sampling System Leak Checks
Time (24 Hr)
Leak Rate, cfm
1 — i^itfoi — I
win
< / C * tin
. oo1^
Final Meter Volume
Initial Meter Volume
Non-sample Volume
Final
(t^5
|(
fffO^
Initial
Final
Initial
Final
Initial
Final
Initial
Final
Remarks and Notes: List any other equipment requiring calibration below.
TRAIN A
M17DPQ1.WPD July 2, 1999
Meter Volume at Start of Run
Meter Volume at End of Run
Total Leak Check Volume
Adjusted Final Volume
-------
Run No.
Date
Sampling Location Unit 2A Baahouse Outlet Duct
Project No. 104951.1.016.05.01
Operator.
page.
of
'2-
Sampling Data for Method M Train A No. M17-A
Traverse
Point
Sampling
Time,
min.
Clock
Time
(24-Hr)
Dry Gas Meter Reading
(VJ, ft3
Initial
Desired
Actual
Velocity
Head
(Ap),
in. H2O
Orifice Pressure
Differential
(AH),
Desired
Actual
Stack
Temp.
ff
/*/
-7
//
(.<*
*-&
/*?
ibol*
0.
C-,02.
/&£
c?
V
6*
-A^
_£_
n.
I
^.yy
o.tf
£±A
t
^L
72-1
~3L
^..7
Z.I
l&L
32^
-2.31
_3L
fO
Q.13
5V
Remarks and Notes:
M17DPG2.WPD July 2, 1999
AP-/-7
RCA#1 APPENDIX C
39
-------
40 CFR 60, APPENDIX A, METHOD 3B
INTEGRATED GAS SAMPLING DATA
Run No. -7
Date
Client/Source U.S. EPA EMC / Coaentrix
Project No. 104951.1.016.05.01
Sample Type (Multi-Point, Single-Point)
Flow Control Device (Valve, Critical Orific
Method 5 Meter Box No.
MSB Pump Type Diaphram
MSB Pump No.
Sampling Location _Unit 2A Baahouse Outlet Duct
Operator _
Bag Type Mylar
Method SB Train No. _
MSB Flow Meter Type.
MSB Flow Meter No.
Sample No.
NA
NA
Rotameter
Desired Sampling Rate _
Leak Check Before Sampling
Total Sampling Time
cc/min
Flow Rate, cc/min: Average
Estimated Total Sample Volume
<3/ After Sampling
min Average Flow Meter Reading
Highest _
Lowest
liters
Time
(24-Hr)
Flow
Meter
Reading
Start
Purge
Start
Sampling
Stop
Sampling
Sampling
Remarks and Notes
-3.0
5.0
1607
((,<#
-3.
(Wo
3.*
M3BSAMP.WPD June 18, 1998
40
RCA#1 APPENDIX C
-------
40 CFR 60, APPENDIX A, METHOD 3B, GAS ANALYSIS BY ORSAT
Run No. '?
Date
•n
o
Project No. 104951.1.016.05.01 Sample No. NA - Train A
Sampling Location Unit 2A Baghouse Outlet Duct
Analysis Start Time
Sample Type (Bag, Grab)
Analyst 0><.
Baa
Orsat Leak Check Before Analysis:
Burrete //O Change in 4 Minutes
Pipettes JV(> Change in 4 Minutes
Orsat Leak Check After Analysis:
Burrete A^ Change in 4 Minutes
Pipettes i#t> Change in 4 Minutes
Analysis
Gas
C02
02 (Net is actual reading
minus actual CO2 reading)
CO (Net is actual reading
minus actual O2 reading)
1
Actual
Reading
1 ;&*
2 ;&iJ
3
1 ;Vz~
2 Jfy,-^
3
1
2
3
Net
Value
/sT , v
. "Z—
2
Actual
Reading
1 /3/P
2 Jjfs &
3
1 ;9-2~
2 ;2-2--
3
1
2
3
Net
Value
JS> &
9.2-
3
Actual
Reading
1 t£'V
2 )g~.i>
3
1 }'
4.2.
Average
Net
Value
(% v/v)
D
y.2-
C02 >4% 0.3% v/v
<4% 0.2% v/v
Acceptance Criteria per Method 3B
02 >15% 0.2% v/v CO
<15% 0.3% v/v
0.3% v/v
Remarks and Notes:
M3BANALWPD May 28. 1999
-------
40 CFR 60, APPENDIX A, METHOD 17 - PARTICULATE MATTER TRAIN (M17)
FIELD LABORATORY TRAIN SET-UP DATA FOR TWO TRAINS
MRI Project No. 104951.1.016.05.01
Client/Source: U.S. EPA OAQPS EMAD EMC / Cogentrix Unit 2A
Source Location: Rocky Mount, North Carolina
Sampling Location: Baghouse (Fabric Filter) Outlet Duct
Run No. '/ Sampling Train A No.
Sampling Train B No. .
Set-up person(s): cA c5/<
Transfer to Sampler:
Relinquished By J
Impinger Outlet Connector
Connector I.D. No.
* Before and after sampling: Nozzle inlet opening and filter assembly holder outlet opening covered with Teflon® tape, and
entire filter assembly holder with filter assembly and nozzle wrapped in aluminum foil and placed in Ziploc* bag. 1st impinger
inlet sealed with glass blank-off.
Comments:
74
M17DSUP.WPD May 13, 1999 (rev. M17DSUP2.WPD July 29, 19991
42
RCA#1 APPENDIX C
-------
40 CFR 60, APPENDIX A, METHOD 17 - PARTICULATE MATTER TRAIN (M17)
FIELD LABORATORY SAMPLE RECOVERY DATA FOR TWO TRAINS
MRI Project No. 104951.1.016.05.01
Client/Source: U.S. EPA OAQPS EMAD EMC / Cogentrix Unit 2A
Source Location: Rocky Mount, North Carolina
Sampling Location: Baghouse (Fabric Filter) Outlet Duct
Run No.
Sampling Train A No.
Sampling Train B No..
Transfer for Recovery:
Relinquished By &> £>r'TT)r
Received By zJ, St.
Impinger Box A No.
Impinger Box B No..
Date/Time
Sample recovery person(s):
Weights below are in grams.
Date:
BACK HALF RECOVERIES
TRAIN A
TRAIN B
Impinger:
Final Wt.
Initial Wt.
Net Wt.
1st
2nd
3rd
4th & 5th
1st
796.1?
2nd
3rd
4th & 5th
Total Condensate Collected:
Description and/or color:
£*'*>-
% Blue
% Blue
FRONT HALF RECOVERIES
TRAIN A
TRAIN B
FILTER ASSEMBLY:
Sample Number: 7102
PM Description/color:
TRAIN RINSES:
Sample Number: ^101
Components Rinsed*: nozzle, filter holder front
•7104
'7103
* Acetone rinses with brushing 3 times or more until perceivably clean.
COMMENTS: Acetone rinses are transferred directly to tared Teflon® beaker liners for analysis.
M17DRCV.WPD May 13, 1999 [rev. M17DRCV2.WPD July 29. 1999)
RCA#1 APPENDIX C
43
-------
FIELD SAMPLING DATA FOR METHOD 17 TRAINS
w
o
Date ---
Run No. V^t—--
Record dala every
Baromeler No. I
minules
Baromelric Pressure
Elevalion to Meter Boxes .
Meter Box Pha, t?t I
in Hg
34 ft
Elevation to Sampling Loc..
in Hg
34 fl
Sampling Location Pba, '2.'?-*0' in Hg
Static Pressure ""^ • &/ in H2O Assumed Moisture
Train A No. M17-A
Probe No. A Lenath: 1 0 ft
Nozzle No. fltf ~(i- Tio Dia. 0,1% in
Pilot Tube No. A C 0.84
Stack Thermocouple No. /( so fit
Filter Holder No. *7
Filter Assembly No. r~V>
Impinaer Box No. /r 2-
Umbilical/lmpinqer Hookup /Xri?^'
Umbilical No. ^J^O '""V
Meter Box No. A^ (°
DGM Correction (Y) (.0/1
Orifice Meter AH@ /,F?2-
Train B No. M17-B
Probe No. B Lenalh: 10 fl
Nozzle No. Atrt~l3 Tio Dia. £>,($*{ in
Pitol Tube No. B Cp 0.84
Slack Thermocouple No.v'^S^D
Filter Holder No. &
Filter Assembly No. LIU
Impinqer Box No. ft 1^
Umbilical/lmpinqer Hookup t^.{T^j2 —
Umbilical No. ft %/-^ /
Meter Box No. /V (I
DGM Correclion (Y) Afl2^
Orifice Meier AH@ /, tyl
page 1 of
Traverse Point Layout
% Assumed %CO,
%02
Time (24 Hr)
Pass or Fail
Time (24 Hr)
Vacuum, in Hg
Leak Rate, cfm
Train A Pilot Tube Pressure Measurement System Leak Checks
Initial
0^0
Final
(((X?
f&kt>
r
Initial
OW
ft
.ooit
Final Meier Volume
Inilial Meier Volume
Leak Check Volume
Initial
Final
Inilial
Final
Final
Krt
\v
fcx
^
Inilial
Inilial
Trait
Final
Initial
Final
i A Sampling System
Final
Inilial
Train B Pilol Tube Pressure Measurement System Leak Checks
Initial
09$
Leak C
Final
1/1$
60A&
Initial
Final
Tiecks
Final
Initial
Initial
Final
Initial
Final
Initial Final
Final
Initial
Final
Time (24 Hr)
Vacuum, in Hg
Leak Rate, cfm
Inilial
ovfr
&
o>tfh
Final Meier Volume"
Inilial Meier Volume
Non-sample Volume
Final
nn
M
*&\
Inilial
Final
Inilial
Final
Inilial
Final
Inilial
Final
Remarks and Noles: Lisl any olher equipment requiring calibration below.
TRAIN A
TRAIN B
Iri
M I/up
-------
Run No.
Date
Sampling Location Unit 2A Baahouse Outlet Duct
Project No. 104951.1.016.05.01 Operator.
page.
of
Sampling Data for Method 17 Train A No. M17-A
Traverse
Point
Sampling
Time,
min.
Clock
Time
(24-Hr)
Dry Gas Meter Reading
(Vm), ft3
Initial
Desired
Actual
Velocity
Head
(Ap),
in. H20
Orifice Pressure
Differential
(AH),
in. H20
Desired
Actual
Stack
Temp.
(U
°F
Dry Gas Meter
Temperature
(tj,
°F
Inlet Outlet
Pump
Vacuum,
in. Hg
Silica Gel
Impinger
Outlet
Temp.,
°F
0
-&
87
-8SL.
JCL
]>-*>
Zff
12-
£&.
/£-
Zc^n
0,82
3L
6,6'?
9?
002.
-&£-
(I
A-?1?
fif-G
II
52^
1010
3SL.
l&fH
/-
(00
-&-
(*>
•2,2-
f.9/
**
/ft
/a
97
i-
toft
2M.$/
•z.
(2-
t-7
M-
•Jo
&
29
/-z-
li-
.ff
0.11
0-t\
l#L
•>.07
C. 5"
&A
40-
100%
JL
34^
4&-
^L
-S$L-
Jeg_
.££-
JDL
MJL
33-
(rti
-U3-
3JL
Co
6.0&
£ r
2-2-
4±5_
±
~K:
•2.1
JSL
Hot
M3-
So
0.1*
j%_
-£4-
Remarks and Notes:
M17DPG2.WPD July 2. 1999
RCA#1 APPENDIX C
45
-------
Date
/
Run No.
Project No.
Sample Type
-------
40 CFR 60, APPENDIX A, METHOD 3B, GAS ANALYSIS BY ORSAT
Run No.
Date
9
o
Project No. 104951.1.016.05.01 Sample No. NA - Train A
Sampling Location Unit 2A Baohouse Outlet Duct
Analysis Start Time
Sample Type (Bag, Grab)
Analyst J.
Bag
Orsat Leak Check Before Analysis:
Burrete /^o Change in 4 Minutes
Pipettes i/VV Change in 4 Minutes
Orsat Leak Check After Analysis:
Burrete /rf Change in 4 Minutes
Pipettes x^7 Change in 4 Minutes
Analysis
Gas
CO2
O2 (Net is actual reading
minus actual C02 reading)
CO (Net is actual reading
minus actual O2 reading)
1
Actual
Reading
1 sg.*-
2 ;&.<£'
3
1 x>#2-
2 /?, Z.
3
1
2
3
Net
Value
Xi>. "Z-
V. V
2
Actual
Reading
1 J&,?-
2 /£VZ-
3
1 y9/z-
2 ;£'2-
3
1
2
3
Net
Value
J&, Z-
4.0
3
Actual
Reading
1 ^Z.
2/^:2,
3
1 /az-
2 >9,-z-
3
1
2
3
Net
Value
/&• Z-
4.O
Average
Net
Value
(% v/v)
J\£>. Z_
•y.o
Acceptance Criteria per Method 3B
C02 > 4% 0.3% v/v O2 >15% 0.2% v/v CO
<4% 0.2% v/v <15% 0.3% v/v
0.3% v/v
Remarks and Notes:
M3BANAL.WPD May 28, 1999
-------
40 CFR 60, APPENDIX A, METHOD 17 - PARTICULATE MATTER TRAIN (M17)
FIELD LABORATORY TRAIN SET-UP DATA FOR TWO TRAINS
MRI Project No. 104951.1.016.05.01
Client/Source: U.S. EPA OAQPS EMAD EMC / Cogentrix Unit 2A
Source Location: Rocky Mount, North Carolina
Sampling Location: Baghouse (Fabric Filter) Outlet Duct
Run No. S Sampling Train A No.
Sampling Train B No.
Set-up person(s): 0,
Impinger Box A No.
Impinger Box B No..
Date:
Transfer to Sampler:
Relinquished By r
Date/Time
TRAIN COMPONENT
REAGENT
LOADING DATA
TRAIN A
TRAIN B
Sampling Nozzle (Quartz)*
Filter Assembly and Holder*
Filter Type: Whatman 934-AH
Probe (316 SS)
Sample Transfer/Vacuum Line
Male 1st Impinger Inlet Blank-Off
Nozzle I.D. No.
Fitter Assembly No.
Filter Holder No-
Initial Weights (grams)
1st Impinger (Mod-GBS) 100-200 mLs ASTM Type I Water
U-Connector (A)
2nd Impinger (GBS) 100-200 mLs ASTM Type I Water
U-Connector (B)
3rd Impinger (Mod-GBS) Empty
U-Connector (C)
4th Impinger (Mod-GBS) "200 g indicating silica gel
U-Connector (D)
5th Impinger (Mod-GBS) /' //
Impinger Outlet Connector
Connector I.D. No.
Before and after sampling: Nozzle inlet opening and filter assembly holder outlet opening covered with Teflon® tape, and
entire filter assembly holder with filter assembly and nozzle wrapped in aluminum foil and placed in Ziploc® bag. 1st impinger
inlet sealed with glass blank-off.
Comments:
M17DSUP.WPD Mav 13. 1999 (rev. M17DSUP2.WPD July 29, 1999)
48
RCA#1 APPENDIX C
-------
40 CFR 60, APPENDIX A, METHOD 17 - PARTICULATE MATTER TRAIN (M17)
FIELD LABORATORY SAMPLE RECOVERY DATA FOR TWO TRAINS
MRI Project No. 104951.1.016.05.01
Client/Source: U.S. EPA OAQPS EMAD EMC / Cogentrix Unit 2A
Source Location: Rocky Mount, North Carolina
Sampling Location: Baghouse (Fabric Filter) Outlet Duct
Run No. S
Sampling Train A No.
Sampling Train B No.
Transfer for Recovery:
Relinquished By &•
Received By
Weights below are in grams.
Date:
BACK HALF RECOVERIES
TRAIN A
TRAIN B
Impinger: 1st
Final Wt.
Initial Wt.
Net Wt.
2nd
3rd
4th & 5th
1st
2nd
3rd
4th & 5th
, /
4.3
Total Condensate Collected:
Description and/or color:
3
Je
% Blue
FRONT HALF RECOVERIES
% Blue
TRAIN A
TRAIN B
FILTER ASSEMBLY:
Sample Number:
PM Description/color:
TRAIN RINSES:
Sample Number:
101
Components Rinsed*: nozzle, filter holder front
* Acetone rinses with brushing 3 times or more until perceivably clean.
COMMENTS: Acetone rinses are transferred directly to tared Teflon® beaker liners for analysis.
M17DRCV.WPO May 13, 1999 (rev. M17DRCV2.WPD July 29, 19991
49
RCA#1 APPENDIX C
-------
en
o
I
o
FIELD SAMPLING DATA FOR METHOD 17 TRAINS
Run No. .
Date
Project No. 104951.1.016.05.01
Client U.S. EPA EMC _
Source Coqentrix Unit 2A _
Sampling Locatio
Operator <
Baahouse Outlet
Record data every
Barometer No.
<~
minutes
Barometric Pressure
Elevation to Meter Boxes
Meter Box Pba,
Elevation to Sampling Loc.
Sampling Location Pbaf
Static Pressure "*
in Hg
34 ft
in Hg
34 ft
. in Hg
Train A No. M17-A
Probe No. A Length: 10 ft
Nozzle No. intf' *) Tip Dia. Orlfa in
Pitot Tube No. A Cp 0.84
Stack Thermocouple No. 'llffr A
Filter Holder No. /
Filter Assembly No. r"fl
Impinaer Box No. A ~(
Umbilical/lmpinger Hookup Li f-t (
Umbilical No. /t/^ ~Y
Meter Box No. A/ 10
DGM Correction (Y) (, -
Train B No. M17-B
Probe No. B Lenath: 10 ft
Nozzle No. ftl1-(r Tip Dia. 0.ft*1 jn
Pitot Tube No. B C 0.84
Stack Thermocouple No. "9/4o K>
Filter Holder No. &-
Filter Assembly No. PI*
Impinqer Box No. (y " f
Umbilical/lmpinger Hookup £fff L~
Umbilical No. fj *r* ~ 1
Meter Box No. N / 1
DGM Correction (Y) /'.O2-3
Orifice Meter AH@ /- ^
Final
|Ht^
OpOA.
Initial
Final
Initial
Final
Initial
Final
Initial
Final
Train B Pitot Tube Pressure Measurement System Leak Checks
Initial
m
Final
m
tH>4A
Initial
Final
Initial
Final
Initial
Final
Initial
Final
Time (24 Hr)
Vacuum, in Hg
Leak Rate, cfm
Initial
II */
1-5
>oov
Final Meter Volume
Initial Meter Volume
Leak Check Volume
Final
\\\o
ll
, rf
,
Final Meter Volume
Initial Meter Volume
Non-sample Volume
Final
HI1
1)
'd
°(
Initial
Final
Initial
Final
Initial
Final
Initial
Final
Remarks and Notes: List any other equipment requiring calibration below.
TRAIN A
i
1///
-------
Run No. T
Date
Sampling Location Unit 2A Baahouse Outlet Duct
page.
of
Project No. 104951.1.016.05.01
Operator.
Sampling Data for Method 17 Train A No. M17-A
Traverse
Point
Sampling
Time,
min.
Clock
Time
(24-Hr)
Dry Gas Meter Reading
(VJ, ft3
Initial
Desired
Actual
Velocity
Head
(Ap),
in. H20
Orifice Pressure
Differential
(AH),
in. H2O
Desired Actual
Stack
Temp.
Dry Gas Meter
Temperature
(tj-
°F
Inlet Outlet
Pump
Vacuum,
in. Hg
Silica Gel
Impinger
Outlet
Temp.,
JLZ_
/-
^£_
_^_
9-?
JZ
•2^,77
&5
57
JfS-
2.-}
*
M3-
.k^L
^
^L
z^j_
H
Ac?
/.f^
?^/- 7^
^./^
^2L
JL
-/-
&-
-U-
-r
Sampling Data for Method 17 Train B No. M17-B
XL
t,,zy
±3>_
•T-
22-
-7
ti-zi
\ji
O.ffr
&*L
M3L
L&-
f-7
ftr~
.Li-
tf.TS
ff
r?
£
4*-
'9
A 7
/a?
JjO*
!•*>
/*/
ft
4*3.
-7
tsn
/oo
T-.o
V
to
f.tl
/oo
5V
LL
AV*
/o
-------
40 CFR 60, APPENDIX A, METHOD 3B
INTEGRATED GAS SAMPLING DATA
Run No.
Date
Client/Source U.S. EPA EMC / Coqentrix
Project No. 104951.1.016.05.01
Sample Type (Multi-Point, Single-Point)
Flow Control Device (Valve, Critical Orifie
Method 5 Meter Box No. /V'/
-------
40 CFR 60, APPENDIX A, METHOD 3B, GAS ANALYSIS BY ORSAT
n
o
Run No.
Date
Project No. 104951.1.016.05.01 Sample No. NA - Train A
Sampling Location Unit 2A Baahouse Outlet Duct
Analysis Start Time /V52?
Sample Type (Bag, Grab)
Analyst J
Baa
Orsat Leak Check Before Analysis:
Burrete A^o Change in 4 Minutes
Pipettes S/o Change in 4 Minutes
Orsat Leak Check After Analysis:
Burrete A£ Change in 4 Minutes
Pipettes Srf? Change in 4 Minutes
Analysis
as
CO2
O2 (Net is actual reading
minus actual CO2 reading)
CO (Net is actual reading
minus actual 02 reading)
1
Actual
Reading
1 Jg,0
2 /&0
3
1 /2Z-
2 /#2_-
3
1
2
3
Net
Value
/5,D
*4:2
2
Actual
Reading
1 j£,0
2 s&Q
3
1 y?,z-
2 S9.Zi.
3
1
2
3
Net
Value
/*fy.O
V-Z~
3
Actual
Reading
1 /JT.tf
2 /'^7C>
3
1 J9.X
2 y^-2-
3
1
2
3
Net
Value
S£T.O
^.&.
Average
Net
Value
(% v/v)
/^3xD
&2-
C02 >4% 0.3% v/v
<4% 0.2% v/v
Acceptance Criteria per Method 3B
O2 £15% 0.2% v/v CO
<15% 0.3% v/v
0.3% v/v
Remarks and Notes:
?/'
en
M3BANAL.WPD May 28, 1999
-------
40 CFR 60, APPENDIX A, METHOD 17 - PARTICULATE MATTER TRAIN (M17)
FIELD LABORATORY TRAIN SET-UP DATA FOR TWO TRAINS
MRI Project No. 104951.1.016.05.01
Client/Source: U.S. EPA OAQPS EMAD EMC / Cogentrix Unit 2A
Source Location: Rocky Mount, North Carolina
Sampling Location: Baghouse (Fabric Filter) Outlet Duct
Run No. 7 Sampling
Sampling
Set-up person(s): \)sSl
Transfer to Sampler:
Relinquished By -J; Svs's?
TRAIN COMPONENT
Train A No. /%!"?-&
Train B No. /2?y?-&
fSrr>^*t
i^si Received By £?•
REAGENT
Impinqer Box A No. /9~J
Impinqer Box B No. f$~~J
Date- &£ -23?-*? 3
&r*TT' *** Date/Time OS-y^'^9 S/OO
LOADING DATA
TRAIN A
TRAIN B
Sampling Nozzle (Quartz)*
Filter Assembly and Holder*
Filter Type: Whatman 934-AH
Probe (316 SS)
Sample Transfer/Vacuum Line
Male 1st Impinger Inlet Blank-Off
Nozzle I.D. No.
Filter Assembly No.
Filter Holder No.
Initial Weights (grams)
1st Impinger (Mod-GBS) 100-200 mLs ASTM Type I Water
U-Connector (A)
2nd Impinger (GBS) 100-200 mLs ASTM Type I Water
U-Connector (B)
3rd Impinger (Mod-GBS) Empty
U-Connector (C)
4th Impinger (Mod-GBS) "200 g indicating silica gel
U-Connector (D)
5th Impinger (Mod-GBS) /> »
Impinger Outlet Connector
Connector I.D. No.
* Before and after sampling: Nozzle inlet opening and filter assembly holder outlet opening covered with Teflon® tape, and
entire filter assembly holder with filter assembly and nozzle wrapped in aluminum foil and placed in Ziploc® bag. 1 st impinger
inlet sealed with glass blank-off.
Comments:
M17DSUP.WPD May 13, 1999 Irev. M17DSUP2.WPD July 29. 19991
54
RCA#1 APPENDIX C
-------
40 CFR 60, APPENDIX A, METHOD 17 - PARTICIPATE MATTER TRAIN (M17)
FIELD LABORATORY SAMPLE RECOVERY DATA FOR TWO TRAINS
MRI Project No. 104951.1.016.05.01
Client/Source: U.S. EPA OAQPS EMAD EMC / Cogentrix Unit 2A
Source Location: Rocky Mount, North Carolina
Sampling Location: Baghouse (Fabric Filter) Outlet Duct
^ Impinger Box A No. ^ ~J
Run No. x Sampling Train A No.
Sampling Train B No. .
Transfer for Recovery:
Relinquished By &' G?SJr*i"* Received By .
Sample recovery person(s): <) «5.
Weights below are in grams.
Impinger Box B No. &~~J
Date/Time
Date:
BACK HALF RECOVERIES
TRAIN A
Impinger: 1st
Final Wt. '793'£~
2nd
3rd
4th & 5th
1st
Initial Wt. &>$&>*)
Net Wt.
J.V
Total Condensate Collected:
Description and/or color:
% Blue
TRAIN B
2nd
3rd
4th & 5th
£,,•2- #./
% Blue
FRONT HALF RECOVERIES
TRAIN A
102
FILTER ASSEMBLY:
Sample Number:
PM Description/color:
TRAIN RINSES:
Sample Number: ^ 101
Components Rinsed*: nozzle, filter holder front
TRAIN B
104
103
* Acetone rinses with brushing 3 times or more until perceivably clean.
COMMENTS: Acetone rinses are transferred directly to tared Teflon® beaker liners for analysis.
M17DRCV.WPD May 13, 1999 (rev. M17DRCV2.WPD July 29, 1999)
RCA#1 APPENDIX C
55
-------
en
FIELD SAMPLING DATA FOR METHOD 17 TRAINS
page 1 of.
Run No. (0 Date
f'tf-ff
Proiect No. 104951.1.016.05.01
Client U.S. EPA EMC
Source Coaentrix Unit 2A
I
fc
'-d
Sampling Locz
Operator
Record data e
Barometer No
Barometric Pr<
Elevation to l\/
Meter Box Pba
Elevation to S
Sampling Locc
Static Pressur
Time (24 Hr)
Pass or Fail
ition Baqhouse Outlet
very T
3ssu(e SJS
eter Boxes
ampling Loc
JtiorhPba, _1
e^3^-^
Train A
Initial Fir
l^inh n
a*
minutes
I/PI in
34
'w'VA in
34
A/W in
& S' in
Hg
ft
Hg
ft
Hg
H2O
Train A No. M17-A
Probe NOj.
Nozzle No
Pitot Tube
Stack The
Filter Hold
Filter Asse
Impinger E
Umbilical/
Umbilical
A Lenath: 10 ft
./Hl7/T-TiDDia.^,/$V in
No. A Cp 0.84
rmocouple No. y'so A
er No. 7
smbly No. ^ '-ft
lox No. /r Z-
mpinaer Hookuo L< n ^O
No. /t/5^~¥
Meter Box No. U [Cf
DGM Correction (Y) (.Oftf
Orifice Meter AH@ IrW^-
Assumed Moisture /T
Train B No.
Probe No.
M17-B
B
Nozzle Noflfy 7 -ft
Pitot Tube f
Stack Therr
Filter Holde
Filter Assen
Impinger'Bc
Umb lical/ln
Umbilical N
>Jo. B
nocouph
rNo.
nbly No.
x No.
ipinger K
0.
Meter Box No.
DGM Correction (Y)
Orifice Meter AH@
3/0 Assumed %CO2 I*
Pitot Tube Pressure Measurement System Leak Checks
ml Initial
11
j.
Final
Initial
Final Initial Final Initial
Final
g / Train A Sampling System
B
n
Time (24 Hr)
Vacuum, in Hg
Leak Rate, cfm
Initial
\*j(j'£\
K
.00$
Final Meter Volume
Initial Meter Volume
Leak Check Volume
Final
/-rn
A
1^
Initial Final Initial
Length: 10 ft
Tip Dia.
>
Hi
£
/'
\
y*
^
^-
7
^ / f s
A P>
Traverse
1
- t
1
U
l/l
LJ LJ Lj
c. "D £
Point Layout
*) %o, y4
Train B Pitot Tube
Initial
\*jo<\
LeakC
Final
(722>
p*iA
necks
Final
Initial
Pressure Measurement System Leak Checks
Final
Initial
Initial
Final
Final
Initial
Final
Initial Final
Initial
Final
Train B Sampling System Leak Checks
Time (24 Hr)
Vacuum, in Hg
Leak Rate, cfm
Initial
\f)(^\
^b
• QC
Final Meter Volume
Initial Meter Volume
Non-sample Volume
7V
Final
i'M-1
[If
,o<$
Initial
Final
Initial
Final
Initial
Final
Initial
Final
Remarks and Notes: List any other equipment requiring calibration below.
fl'll*
M17DPG1.WPD July 2, 1999
Meter Volume at Start of Run
Meter Volume at End of Run
Total Leak Check Volume
Adjusted Final Volume
TRAIN A
, rtt
-------
Run No.
Date
Sampling Location Unit 2A Baahouse Outlet Duct
Project No. 104951.1.016.05.01
Operator.
page.
Sampling Data for Method 17 Train A No. M17-A
Traverse
Point
Sampling
Time,
min.
Clock
Time
(24-Hr)
Dry Gas Meter Reading
(VJ, ft3
Initial
Desired
Actual
Velocity
Head
(Ap),
Orifice Pressure
Differential
(AH),
Desired Actual
Stack
Temp.
8
ff.6*
sal
(drt
/a/
2-7
IL2.I
. 2.7
o.cn-
/0V
I.9L
*
2 r
ff
p. 17.
6.58
fol-
ft
2.
2.01
^i-
1.0
SL
I
-L,0
53
01$-
0-lt,
O.H,
1£L
Is^.
3-
J3L
Remarks and Notes:
M17DPG2.WPD July 2, 1999
RCA#1 APPENDIX C
57
-------
40 CFR 60, APPENDIX A, METHOD 3B
INTEGRATED GAS SAMPLING DATA
Run No.
Date
Client/Source U.S. EPA EMC / Coaentrix
Project No. 104951.1.016.05.01
Sample Type (Multi-Point, Gingle-Point)
Flow Control Device (Valve, Critical Orifice)
Method 5 Meter Box No.
MSB Pump Type Diaphram
MSB Pump No.
Sampling Location Unit 2A Baahouse Outlet Duct
Operator
Bag Type Mylar
Method SB Train No.
MSB Flow Meter Type
MSB Flow Meter No.
Sample No.
NA _
NA
Rotameter
Desired Sampling Rate
Leak Check Before Sampling
Total Sampling Time
cc/min
Flow Rate, cc/min: Average
Estimated Total Sample Volume
> After Sampling
min Average Flow Meter Reading
^"^^ Highest
Lowest
liters
Time
(24-Hr)
Flow
Meter
Reading
Start
Purge
Start
Sampling
Stop
Sampling
Sampling
Remarks and Notes
l-ftf
/fff
•3.0
C/
•5.0
J.o
S-c
•?>.<=
(Irfr
"5.0-
3.°
10
M3BSAMP.WPD June 18, 1998
58
RCA#1 APPENDIX C
-------
40 CFR 60, APPENDIX A, METHOD 3B, GAS ANALYSIS BY ORSAT
Run No. /£>
Date
I
m
o
Project No. 104951.1.016.05.01 Sample No. NA - Train A
Sampling Location Unit 2A Baahouse Outlet Duct
Analysis Start Time
Sample Type (Bag, Grab)
Analyst J i
Baa
Orsat Leak Check Before Analysis:
Burrete Wo Change in 4 Minutes
Pipettes //o Change in 4 Minutes
Orsat Leak Check After Analysis:
Burrete /Vv Change in 4 Minutes
Pipettes f/Q Change in 4 Minutes
Analysis
Gas
CO2
O2 (Net is actual reading
minus actual C02 reading)
CO (Net is actual reading
minus actual 02 reading)
1
Actual
Reading
1 j£,'3.
2 /£~/2-
3
1 /22
2 j9,2-
3
1
2
3
Net
Value
,X£72--
f/:O
2
Actual
Reading
1 Jf.-i-
2 /£*-
3
1 rt.-z.
2 J9/2-
3
1
2
3
Net
Value
A5, 2-
4-.O
3
Actual
Reading
1 ,^",2.
2 /£:z-
3
1 /£2-
2 ;9.-z-
3
1
2
3
Net
Value
>>J^:2
$>,O
Average
Net
Value
(% v/v)
/5S^~
4O
Acceptance Criteria per Method 3B
C02 >4% 0.3% v/v
<4% 0.2% v/v
02 £15% 0.2% v/v
<15% 0.3% v/v
CO 0.3% v/v
Remarks and Notes:
on
CO
M3BANAL.WPD May 28, 1999
-------
40 CFR 60, APPENDIX A, METHOD 17 - PARTICULATE MATTER TRAIN (M17)
FIELD LABORATORY TRAIN SET-UP DATA FOR TWO TRAINS
MRI Project No. 104951.1.016.05.01
Client/Source: U.S. EPA OAQPS EMAD EMC / Cogentrix Unit 2A
Source Location: Rocky Mount, North Carolina
Sampling Location: Baghouse (Fabric Filter) Outlet Duct
Impinger Box A No.
Impinger Box B No..
8
Run No. /£> Sampling Train A No.
Sampling Train B No.
Set-up person(s): J . £tfs's7r^?s?
Transfer to Sampler:
Relinquished By J . £vs'jm£si Received By
Date:
Date/Time
TRAIN COMPONENT
REAGENT
LOADING DATA
TRAIN A
TRAIN B
Sampling Nozzle (Quartz)*
Filter Assembly and Holder*
Filter Type: Whatman 934-AH
Probe (316 SS)
Sample Transfer/Vacuum Line
Male 1st Impinger Inlet Blank-Off
Nozzle l.D. No.
Filter Assembly No.
Filter Holder No.
1st Impinger (Mod-GBS) 100-200 mLs ASTM Type I Water
U-Connector (A)
2nd Impinger (GBS) 100-200 mLs ASTM Type I Water
U-Connector (B)
3rd Impinger (Mod-GBS) Empty
U-Connector (C)
4th Impinger (Mod-GBS) "200 g indicating silica gel
U-Connector (D)
5th Impinger (Mod-GBS) n >/
Impinger Outlet Connector
Connector l.D. No.
Initial Weights (grams)
* Before and after sampling: Nozzle inlet opening and filter assembly holder outlet opening covered with Teflon® tape, and
entire filter assembly holder with filter assembly and nozzle wrapped in aluminum foil and placed in Ziploc® bag. 1st impinger
inlet sealed with glass blank-off.
Comments:
M17DSUP.WPD May 13, 1999 (rev. M17DSUP2.WPD July 29, 19991
60
RCA#1 APPENDIX C
-------
40 CFR 60, APPENDIX A, METHOD 17 - PARTICULATE MATTER TRAIN (M17)
FIELD LABORATORY SAMPLE RECOVERY DATA FOR TWO TRAINS
MRI Project No. 104951.1.016.05.01
Client/Source: U.S. EPA OAQPS EMAD EMC / Cogentrix Unit 2A
Source Location: Rocky Mount, North Carolina
Sampling Location: Baghouse (Fabric Filter) Outlet Duct
Run No. /& Sampling Train A No.
Sampling Train B No.
Transfer for Recovery:
Relinquished By V> &*,&> s> _ Received By 101
Components Rinsed*: nozzle, filter holder front
TRAIN B
* Acetone rinses with brushing 3 times or more until perceivably clean.
COMMENTS: Acetone rinses are transferred directly to tared Teflon® beaker liners for analysis.
1J,
M17DRCV.WPD May 13, 1999 (rev. M17DBCV2.WPD July 29. 19991
RCA#1 APPENDIX C
61
-------
ro
*
m
n
FIELD SAMPLING DATA FOR METHOD 17 TRAINS
Run No. //
Date
Project No. 104951.1.016.05.01
Client U.S. EPA EMC
Source Coaentrix Unit 2A
Sampling Location. Baahouse Outlet
Operator ^
Record data every
Barometer No.
minutes
Barometric Pressure "2
Elevation to Meter Boxes
Meter Box Pba,
- "72-
in Hg
34 ft
Elevation to Sampling Loc..
jtt
Sampling Location^,,
Static Pressure'
\n Hg
34 ft
. in Hg
Train A No. M17-A
Probe No. A Lenath: 1 0 ft
Nozzle No./^'7"5 Tip Dia. 0-1^ in
Pitot Tube No. A CD 0.84
Stack Thermocouole No. "2138 /(
Filter Holder No. £~
Filter Assembly No. i^-l
Impinaer Box No. A~l
Umbilical/lmDinqer Hookutfi-ASfa^-^U/
Umbilical No. fjfa'i
Meter Box No. A//0
DGM Correction (Y) /. otf
Orifice Meter AH@ /-$"32-
Train B No. M17-B
Probe No. B Lenath: 10 ft
Nozzle No. JMI7-4- Tip Dia. ^'fti in
Pitot Tube No. B CD 0.84
Stack Thermocouple No. <3/5'"~ 1
Umbilical/lmoinqer Hookup LjlJ 2^-
Umbilical No. A/^-/
Meter Box No. A///
DGM Correction (Y) /< 02-3
Orifice Meter AH@ A *?
Initial
Final
Initial
Final
Initial
Final
Initial
Final
Train B Pitot Tube Pressure Measurement System Leak Checks
Initial
oWt
Final
(Vfi
p(Xjd
Initial
Final
Initial
Final
Initial
Final
Initial
Final
Train A Sampling System Leak Checks
Time (24 Hr)
Vacuum, in Hg
Leak Rate, cfm
Initial
w
tf
,0t>l.
Final Meter Volume
Initial Meter Volume
Leak Check Volume
Final
[IV\
<\
,001
Initial
Final
Initial
Final
Initial
Final
Initial
Final
Time (24 Hr)
Vacuum, in Hg
Leak Rate, cfm
Initial
Wo
15 i
10*4
Final Meter Volume
Initial Meter Volume
Non-sample Volume
Final
\^n
(0
•n
&
Initial
Final
Initial
Final
Initial
Final
Initial
Final
Remarks and Notes: List any other equipment requiring calibration below.
TRAIN A
M17DPG1.WPD July 2, 1999
Meter Volume at Start of Run
Meter Volume at End of Run
Total Leak Check Volume
Adjusted Final Volume
TRAIN B
"MS
V
-------
Run No.
Date
Sampling Location Unit 2A Baahouse Outlet Duct
Project No. 104951.1.016.05.01
Operator
page.
of
Sampling Data for Method 17 Train A No. M17-A
Traverse
Point
Samplinc
Time,
Clock
Time
(24-Hr)
Dry Gas Meter Reading
(VJ, ft3
Initial
Desired
Actual
Velocity
Head
(Ap),
in. H20
Orifice Pressure
Differential
(AH),
Desired
Actual
Stack
Temp.
33_
UL.
22^
IIVI-
i*
2,2-
^£.
12-
foe, el
128L
98
33-
£2-
£L
aw
0,13
•2->
ffz-
72-
/**/
1-3
£L
9*
f?
/
^5.
v
ft-
fell
. 77
AZ
5~
Samplinq Data for Method 17 Train B No. M17-B
A-f
^_
^2_
72-
±£L
£JL
72-
fort
1,0
'73
JZL
iSL
it&L
VM
20
^7-^
^/?.V/
^_
f-b
ASO-
{.?&
57
_y_
Zf
//g;-
.2=L
2L
^21
3
•fe.
z
~T
11(0
wi.
^
vn.it.
A?
till
100.
f.1
(X
flZ-f
Remarks and Notes:
M17DPG2.WPD July 2. 1999
~
RCA#1 APPENDIX C
63
-------
40 CFR 60, APPENDIX A, METHOD 3B
INTEGRATED GAS SAMPLING DATA
Run No. //
Date
Client/Source U.S. EPA EMC / Cooentrix
Project No. 104951.1.016.05.01
Sample Type (Multi-Point, Single-Point)
Flow Control Device (Valve, Critical Orifi
Method 5 Meter Box No.
MSB Pump Type Diaohram
MSB Pump No.
Sampling Location Unit 2A Baahouse Outlet Duct
Operator &irt4J-~^-
Bag Type Mvlar
Method SB Train No._
MSB Flow Meter Type
MSB Flow Meter No.
Sample No.
NA
NA
Rotameter
Desired Sampling Rate
Leak Check Before Sampling.
Total Sampling Time
cc/min
Flow Rate, cc/min: Average
Estimated Total Sample Volume
& After Sampling
min Average Flow Meter Reading
Highest ~?'rc
Lowest
liters
Time
(24-Hr)
Flow
Meter
Reading
Start
Purge
Start
Sampling
Stop
Sampling
Sampling
Remarks and Notes
1.0
CS
(fol
ft/2-
f/W
It IS
tn?
(2-lt
M3BSAMP.WPD June 18, 1998
64
RCA#1 APPENDIX C
-------
40 CFR 60. APPENDIX A, METHOD 3B, GAS ANALYSIS BY ORSAT
Run No. /S
Date
n
n
Project No. 104951.1.016.05.01 Sample No. NA - Train A
Sampling Location Unit 2A Baghouse Outlet Duct
Analysis Start Time
Sample Type (Bag, Grab)
Analyst
y.fr
3
Actual
Reading
1 /#o
2 J *S,t}
3
1 J fr fr
' /i5 'v
2 yp'J^
3
1
2
3
Net
Value
J V.O
^.fr
Average
Net
Value
(% v/v)
S4*. 0
$*••&
Acceptance Criteria per Method 3B
C02 > 4% 0.3% v/v O2 >15% 0.2% v/v CO
<4% 0.2% v/v
0.3% v/v
<15% 0.3% v/v
Remarks and Notes:
OJ
en
M3BANAL.WPD May 28. 1999
-------
40 CFR 60, APPENDIX A, METHOD 17 - PARTICULATE MATTER TRAIN (Ml 7)
FIELD LABORATORY TRAIN SET-UP DATA FOR TWO TRAINS
MRI Project No. 104951.1.016.05.01
Client/Source: U.S. EPA OAQPS EMAD EMC / Cogentrix Unit 2A
Source Location: Rocky Mount, North Carolina
Sampling Location: Baghouse (Fabric Filter) Outlet Duct
Run No. /J Sampling Train A No.
Sampling Train B No.
Set-up person(s):
Transfer to Sampler:
Impinger Box A No. >/9*~J
Impinger Box B No. <&~J
Date:
Relinquished By J •
Received By £?• <£/-./ H~' r->
Date/Time
TRAIN COMPONENT
REAGENT
LOADING DATA
TRAIN A
TRAIN B
Sampling Nozzle (Quartz)*
Filter Assembly and Holder*
Filter Type: Whatman 934-AH
Probe (31 6 SS)
Sample Transfer/Vacuum Line
Male 1st Impinger Inlet Blank-Off
Nozzle I.D. No.
Fitter Assembly No.
Filter Holder No.
Initial Weights (grams)
1st Impinger (Mod-GBS) 100-200 mLs ASTM Type I Water
U-Connector (A)
2nd Impinger (GBS) 100-200 mLs ASTM Type I Water
U-Connector (B) K
3rd Impinger (Mod-GBS) Empty
U-Connector (C)
4th Impinger (Mod-GBS) "200 g indicating silica gel
U-Connector (D)
5th Impinger (Mod-GBS) " //
Impinger Outlet Connector
Connector I.D. No.
Before and after sampling: Nozzle inlet opening and filter assembly holder outlet opening covered with Teflon® tape, and
entire filter assembly holder with filter assembly and nozzle wrapped in aluminum foil and placed in Ziploc® bag. 1st impinger
inlet sealed with glass blank-off.
Comments:
M17DSUP.WPD May 13, 1999 Irev. M17DSUP2.WPD July 29, 19991
66
RCA#1 APPENDIX C
-------
40 CFR 60, APPENDIX A, METHOD 17 - PARTICULATE MATTER TRAIN (M17)
FIELD LABORATORY SAMPLE RECOVERY DATA FOR TWO TRAINS
MRI Project No. 104951.1.016.05.01
Client/Source: U.S. EPA OAQPS EMAD EMC / Cogentrix Unit 2A
Source Location: Rocky Mount, North Carolina
Sampling Location: Baghouse (Fabric Filter) Outlet Duct
Run No.
Sampling Train A No.
Sampling Train B No.
Transfer for Recovery:
Relinquished By £?•
Received By J'.
Impinger Box A No.
Impinger Box B No.
Date/Time
Sample recovery person(s):
Weights below are in grams.
Date:
BACK HALF RECOVERIES
TRAIN A
Impinger: 1st
Final Wt. '7*7,9
2nd
3rd
4th & 5th
1st
Initial Wt. &47, t>
Net Wt. /Vfl.?
Total Condensate Collected:
Description and/or color:
% Blue
TRAIN B
2nd
3rd
63*3
^.6 ~0.t
4th & 5th
/(*>#•!>
% Blue
FRONT HALF RECOVERIES
TRAIN A
TRAIN B
FILTER ASSEMBLY:
Sample Number:
PM Description/color: tj&
TRAIN RINSES:
Sample Number: //101
Components Rinsed*: nozzle, filter holder front
//103
* Acetone rinses with brushing 3 times or more until perceivably clean.
COMMENTS: Acetone rinses are transferred directly to tared Teflon® beaker liners for analysis.
<9A
M17DRCV.WPD May 13, 1999 (rev. M17DRCV2.WPD July 29, 1999)
RCA#1 APPENDIX C
67
-------
Oi
CO
n
£
i
o
FIELD SAMPLING DATA FOR METHOD 17 TRAINS
Run No.
Date
Project No. 104951.1.016.05.01
Client U.S. EPA EMC
Source Cogentrix Unit 2A
Sampling Location
Operator
Baohouse Outlet
Record data every
Barometer No.
minutes
Barometric Pressure "2-1-1*1 in Hg
Elevation to Meter Boxes _ 34 ft
Meter Box Pbar *• '
Elevation to Sampling Loc.
Sampling Location Pbar 7^''
Static Pressure
; inHg
34 ft
in Hg
Train A No. M17-A
Probe No. A Length: 10 ft
Nozzle No. fWl'J* 11- Tip Dia. 0 • /£% in
Pitot Tube No. A CD 0.84
Stack Thermocouple No. ^v5y-/&-
Filter Holder No. 1
Filter Assembly No. f~ i-7
Imoinqer Box No. A '2--
Umbilical/lmpinqer Hookup Ufa ty
Umbilical No. tJ "TO ~H"
Meter Box No. AJ (ri
DGM Correction (Y) l> 0 l°l
Orifice Meter AH@ /.ftll^
Train B No. M17-B
Probe No. B Lenqth: 1 0
Nozzle No. A1/X?> Tip Dia. O.fa1!
Pitot Tube No. B CD 0.84
Stack Thermocouple No. ^C^^
Filter Holder No. ft
Filter Assembly No. f-Ztf
Imoinqer Box No. /3^"
Umbilical/lmpinaer Hookup f^lf ^^
Umbilical No. /J^> -'
_ft
in
Meter Box No. A/-/ 1
DGM Correction (Y) /,^^3
Orifice Meter AH@ /, tf/
page 1 of.
A P? C. p fc
Traverse Point Layout
Assumed Moisture
% Assumed %CO2
Time (24 Hr)
Pass or Fail
Train A Pitot Tube Pressure Measurement System Leak Checks
Initial
\t)(»
Initial
Final
Initial
Final
Initial
Final
Initial
Final
Remarks and Notes: List any other equipment requiring calibration below.
TRAIN A
ill
M17DPQ1.WPD July 2, 1999
Meter Volume at Start of Run
Meter Volume at End of Run
Total Leak Check Volume
Adjusted Final volume
-------
Run No.
Date
Sampling Location Unit 2A Baahouse Outlet Duct
Project No. 104951.1.016.05.01
Operator.
page.
of
Sampling Data for Method 17 Train A No. M17-A
Sampling
Time,
Traverse
Point
Clock
Time
(24-Hr)
Dry Gas Meter Reading
(VJ, ft3
Initial
Desired
Actual
Velocity
Head
(Ap),
in. H20
Orifice Pressure
Differential
(AH),
in. H20
Desired Actual
Stack
Temp.
(ts),
°F
Dry Gas Meter
Temperature
Inlet
Outlet
Pump
Vacuum,
in. Hg
Silica Gel
Impinger
Outlet
Temp.,
°F
c-f
&-
z^L
7V
JL.
H%.fj
2^JL
9
ff
7?
20
£.02-
.$•
WLfS
ffc-
2?
72-
l*3£-
ff/
2-
&.8S
-7-r
0. 07
^=£_
2.C2-
7$
ft.
-7*
fl
AZ_
/.v
47
-2.1
Z-/
7?
fl
M-
2JL
2.22.
•2.2-
f/
72.
Xf/
/-f
tf
f'1
(J57
0,23
7*
&3L
Z-l
77
XZ-
J^_
Z-"
-7-7
6. 95
#2.
9-f
•76
Sampling Data for Method 1 7 Train B No. M17-B
•?<$'<#
2.7
7?
77
/z-
31U
37_
2^-
Z.O
-78-
vy
T7
'&.
2£L.
o.To
71
•720.
2.
I'M-
8t>
&
(Z.
^
im
M.
/^L
7V
lit.
•?2&,
ff.tl
y?
Z.t
J2-
7?
JJL
z.tf
8-2-
7?
/Z-
Z.o
7.7/,»/
, i- -w f I
•711, if
an
6.
-------
40 CFR 60, APPENDIX A, METHOD 3B
INTEGRATED GAS SAMPLING DATA
Run No.
Date
Client/Source U.S. EPA EMC / Coaentrix
Project No. 104951.1.016.05.01
Sample Type (Multi-Point, Single-Point)
Flow Control Device (Valve, Critical Orifice)
Method 5 Meter Box No..
MSB Pump Type Diaphram
MSB Pump No._
Sampling Location Unit 2A Baahouse Outlet Duct
Operator ^r^9^—
Bag Type Mvlar Sample No. NA
fl/l*
Method SB Train No. _
MSB Flow Meter Type
MSB Flow Meter No.
NA
Rotameter
Desired Sampling Rate /g
Leak Check Before Sampling.
Total Sampling Time .
Q /I
70
RCA#1 APPENDIX C
-------
40 CFR 60, APPENDIX A, METHOD 3B, GAS ANALYSIS BY ORSAT
Date 0J>~3C>
I
t—«
I
o
Run No.
Project No. 104951.1.016.05.01 Sample No. NA - Train A
Sampling Location Unit 2A Baghouse Outlet Duct
Analysis Start Time /V^
Sample Type (Bag, Grab)
Analyst «J,
Bag
Orsat Leak Check Before Analysis:
Burrete ^p Change in 4 Minutes
Pipettes Wv Change in 4 Minutes
Orsat Leak Check After Analysis:
Burrete S*(> Change in 4 Minutes
Pipettes -^D Change in 4 Minutes
Analysis
Gas
CO2
O2 (Net is actual reading
minus actual C02 reading)
CO (Net is actual reading
minus actual 02 reading)
1
Actual
Reading
1 '&
2 /*>'$
3
1 /£>«•
2 /?.y>
3
1
2
3
Net
Value
/ •£
x57/
2
Actual
Reading
- i jj •*?
o § ^^ "7
3
1 ;9-y
2 /^V
3
1
2
3
Net
Value
/y-->
cSV
3
Actual
Reading
1 ^V/7
2 //y> ^
Average
Net
Value
(% v/v)
/vjr
&>)
Acceptance Criteria per Method 3B
C02 >4% 0.3% v/v O2 >15% 0.2% v/v CO
<4% 0.2% v/v <15% 0.3% v/v
0.3% v/v
Remarks and Notes:
M3BANAL.WPD May 28, 1999
-------
40 CFR 60, APPENDIX A, METHOD 17 - PARTICULATE MATTER TRAIN (M17)
FIELD LABORATORY TRAIN SET-UP DATA FOR TWO TRAINS
MRI Project No. 104951.1.016.05.01
Client/Source: U.S. EPA OAQPS EMAD EMC / Cogentrix Unit 2A
Source Location: Rocky Mount, North Carolina
Sampling Location: Baghouse (Fabric Filter) Outlet Duct
Run No.
Sampling Train A No.
Sampling Train B No.
Impinger Box A No.
Impinger Box B No..
Set-up person(s): _
Transfer to Sampler:
Relinquished By •J •
Date:
TRAIN COMPONENT
Received By
REAGENT
Sampling Nozzle (Quartz)*
Filter Assembly and Holder*
Filter Type: Whatman 934-AH
Probe (316 SS)
Sample Transfer/Vacuum Line
Male 1st Impinger Inlet Blank-Off
Date/Time 0P-30-
LOADING DATA
TRAIN A
TRAIN B
Nozzle I.D. No.
Filter Assembly No.
Filter Holder No.
Initial Weights (grams)
1st Impinger (Mod-GBS) 100-200 mLs ASTM Type I Water
U-Connector (A)
2nd Impinger (GBS) 100-200 mLs ASTM Type t Water
U-Connector (B)
3rd Impinger (Mod-GBS) Empty
U-Connector (C)
4th Impinger (Mod-GBS) "200 g indicating silica gel
U-Connector (D)
5th Impinger (Mod-GBS) /> //
t£>
Impinger Outlet Connector
Connector I.D. No.
* Before and after sampling: Nozzle inlet opening and filter assembly holder outlet opening covered with Teflon® tape, and
entire filter assembly holder with filter assembly and nozzle wrapped in aluminum foil and placed in Ziploc® bag. 1st impinger
inlet sealed with glass blank-off.
Comments:
?///?'
M17DSUP.WPD May 13. 1999 (rev. M17DSUP2.WPD July 29. 1999)
72
RCA#1 APPENDIX C
-------
40 CFR 60, APPENDIX A, METHOD 17 - PARTICULATE MATTER TRAIN (M17)
FIELD LABORATORY SAMPLE RECOVERY DATA FOR TWO TRAINS
MRI Project No. 104951.1.016.05.01
Client/Source: U.S. EPA OAQPS EMAD EMC / Cogentrix Unit 2A
Source Location: Rocky Mount, North Carolina
Sampling Location: Baghouse (Fabric Filter) Outlet Duct
Run No.
Sampling Train A No.
Sampling Train B No..
Impinger Box A No.
Impinger Box B No..
Transfer for Recovery:
Relinquished By £?• £>fj-}'rjr> _ Received By J. .^i
Sample recovery person(s): *Ji
Weights below are in grams.
Date/Time
Date:
BACK HALF RECOVERIES
TRAIN A
Impinger:
Final Wt.
Initial Wt.
Net Wt.
1st
2nd
3rd
, 8
4th & 5th
1st
£5377
Total Condensate Collected:
Description and/or color:
% Blue
TRAIN B
2nd
3rd
4th & 5th
% Blue
FRONT HALF RECOVERIES
TRAIN A
TRAIN B
FILTER ASSEMBLY:
Sample Number:
PM Description/color:
TRAIN RINSES:
Sample Number:
Components Rinsed*: nozzle, filter holder front
* Acetone rinses with brushing 3 times or more until perceivably clean.
COMMENTS: Acetone rinses are transferred directly to tared Teflon® beaker liners for analysis.
IT"
M17DRCV.WPD May 13. 1999 (rev. M17DRCV2.WPD July 29. 19991
RCA#1 APPENDIX C
73
-------
RCA #1 Appendix D
M17 Field Laboratory Particulate Weight Data
MRJ-OPPT\R4703-02-07 Appendices Covers WPD
-------
PARTICULATE MATTER (FRONT-HALF) RINSES ANALYSIS DATA
MRI Project No. 104951.1.016.05.01
Client/Source: U.S. EPA OAQPS EMAD EMC / Cogentrix Unit 2A
Source Location: Rocky Mount, North Carolina
Sampling Location: Baghouse (Fabric Filter) Outlet Duct
Sampling Team Leader: Jim Surman Analyst:
Beaker Liner Size and Type: 250-mL Teflon®
Acetone Lot No. BO 363
Sample Treatment: Acetone samples evaporated at ambient temperature and pressure in an
enclosure with HEPA-filtered air; then, desiccated and weighed to a constant weight.
Weight Unit: grams
Run No. / & Beaker No. f Sample No. .
Sample Volume + Acetone Rinses of Bottle Beaker Liner + Sample Residue Weights
^ Gross Wt. Date Time
Beaker + Liner + Sample + Rinses Wt.
Beaker + Liner Tare Wt.
Sample + Rinses Wt.
Acetone Wt./0.79 = mLs Acetone:
Beaker Liner + Residue Gross Weight used for data entry:
Beaker Liner Tare Weight from Tare Weight Data: 3- "•>
Acetone Blank for data entry = @_ mg/mL
Volume for data entry = ^^."7 mLs
Comments:
Run No. / 8 Beaker No. ^? Sample No.
Sample Volume + Acetone Rinses of Bottle - Beaker Liner + Sample Residue Weights
Gross Wt. Date Time
I —• J+ ^"t
Beaker + Liner + Sample + Rinses Wt.
Beaker + Liner Tare Wt.
Sample + Rinses Wt.
Acetone Wt./0.79 = mLs Acetone:
Beaker Liner + Residue Gross Weight used for data entry:
Beaker Liner Tare Weight from Tare Weight Data:
Acetone Blank for data entry = O_ mg/mL
Volume for data entry = •3?Ajf mLs
Comments:
Run No. Zctr? Beaker No. o Sample No.
Sample Volume + Acetone Rinses of Bottle Beaker Liner + Sample Residue Weights
Gross Wt. Date Time
._•« ^fm ._
Beaker + Liner + Sample + Rinses Wt.
Beaker + Liner Tare Wt.
Sample + Rinses Wt.
Acetone Wt./0.79 = mLs Acetone:
Beaker Liner + Residue Gross Weight used for data entry:
Beaker Liner Tare Weight from Tare Weight Data:
Acetone Blank for data entry = O mg/mL
Volume for data entry = ZP3-'3 mLs
Comments:
NOTE: Control liner and reagent blank weight data and balance check data are documented on other forms.
M5IPMRIX.WPD June 5, 1998 (rev. M17PMRI2.WPD July 29, 1999)
RCA#1 APPENDIX D
-------
PARTICULATE MATTER (FRONT-HALF) RINSES ANALYSIS DATA
MRI Project No. 104951.1.016.05.01
Client/Source: U.S. EPA OAQPS EMAD EMC / Cogentrix Unit 2A
Source Location: Rocky Mount, North Carolina
Sampling Location: Baghouse (Fabric Filter) Outlet Duct
Sampling Team Leader: Jim Surman Analyst:
Beaker Liner Size and Type: 250-mL Teflon® f f
Acetone Lot No. BO 363
Sample Treatment: Acetone samples evaporated at ambient temperature and pressure in an
enclosure with HEPA-filtered air; then, desiccated and weighed to a constant weight.
Weight Unit: grams
Run No. at* & Beaker No. *r Sample No.
Sample Volume + Acetone Rinses of Bottle Beaker Liner + Sample Residue Weights
Gross Wt. Date Time
Beaker + Liner + Sample + Rinses Wt. /£:3'U> 3-'.
Beaker + Liner Tare Wt. S&3-3. 3> •?/&*>
Sample + Rinses Wt. /9V
Acetone Wt./0.79 = mLs Acetone:
Beaker Liner + Residue Gross Weight used for data entry: "3.'
Beaker Liner Tare Weight from Tare Weight Data:
Acetone Blank for data entry = t? mg/mL
Volume for data entry = £?&£• mLs
Comments:
Run No. 3& Beaker No. ^^? Sample No. 3S£/
Sample Volume + Acetone Rinses of Bottle Beaker Liner + Sample Residue Weiahts
Gross Wt. Date Time
_ _^* .,
Beaker + Liner + Sample + Rinses Wt.
Beaker + Liner Tare Wt.
Sample + Rinses Wt. ,
Acetone Wt./0.79 = mLs Acetone:
Beaker Liner + Residue Gross Weight used for data entry:
Beaker Liner Tare Weicjhtifrom Tare Weight Data:
Acetone Blank for data entry = Q_ mg/mL
Volume for data entry = S'?--^?' mLs
Comments:
Run No. oo Beaker No. fe Sample No.
Sample Volume + Acetone Rinses of Bottle Beaker Liner + Sample Residue Weiahts
Gross Wt. Date Time
Beaker + Liner + Sample + Rinses Wt. /V#V &'.
Beaker + Liner Tare Wt.
Sample + Rinses Wt.
Acetone Wt./0.79 = mLs Acetone: 33••
Beaker Liner + Residue Gross Weight used for data entry: 3,'.
Beaker Liner Tare Weight from Tare Weight Data:
Acetone Blank for data entry = 0_ mg/mL
Volume for data entry = 33>"£. mLs
Comments:
NOTE: Control liner and reagent blank weight data and balance check data are documented on other forms.
M5IPMRIX.WPO June 5, 1998 (rev. M17PMRI2.WPD July 29. 1999)
RCA#1 APPENDIX D
-------
PARTICULATE MATTER (FRONT-HALF) RINSES ANALYSIS DATA
MRI Project No. 104951.1.016.05.01
Client/Source: U.S. EPA OAQPS EMAD EMC / Cogentrix Unit 2A
Source Location: Rocky Mount, North Carolina
Sampling Location: Baghouse (Fabric Filter) Outlet Duct
Sampling Team Leader: Jim Surman Analyst: ^/^
Beaker Liner Size and Type: 250-mL Teflon® ' ^
Acetone Lot No. BO 363
Sample Treatment: Acetone samples evaporated at ambient temperature and pressure in an
enclosure with HEPA-filtered air; then, desiccated and weighed to a constant weight.
Weight Unit: grams
Run No. V/r Beaker No. "7 Sample No.
Sample Volume + Acetone..Rjn_sgs_pf Bottle Beaker Liner + Sample Residue Weights
Gross Wt. Date Time
Beaker + Liner + Sample + Rinses Wt.
Beaker + Liner Tare Wt. «%^'7 3;
Sample + Rinses Wt.
Acetone Wt./0.79 = mLs Acetone:
Beaker Liner + Residue Gross Weight used for data entry: 3;
Beaker Liner Tare Weight from Tare Weight Data: 3.
Acetone Blank for data entry = O mg/mL
Volume for data entry = 2?^ 3 mLs
Comments:
Run No. V&> Beaker No. 5 Sample No.
Sample Volume + Acetone Rinses of Bottle Beaker Liner + Sample Residue Weights
_. . Gross Wt. Date Time
Beaker + Liner + Sample + Rinses Wt.
Beaker + Liner Tare Wt. J&& J
Sample + Rinses Wt.
Acetone Wt./0.79 = mLs Acetone:
Beaker Liner + Residue Gross Weight used for data entry:
Beaker Liner Tare Weight from Tare Weight Data:
Acetone Blank for data entry = , & mg/mL
Volume for data entry = &sff{9. '3 " mLs
Comments:
Run No. 0>*7 Beaker No. 7 Sample No.
Sample Volume + Acetone Rinses of Bottle Beaker Liner + Sample Residue Weights
Gross Wt. Date Time
Beaker + Liner + Sample + Rinses Wt. /-££ 7 3^ i
Beaker + Liner Tare Wt. //^.f' 3 4%gV 0/ ffQ-99
Sample + Rinses Wt.
Acetone Wt./0.79 = mLs Acetone:
Beaker Liner + Residue Gross Weight used for data entry:
Beaker Liner Tare Weight from Tare Weight Data:
Acetone Blank for data entry = & mg/mL
Volume for data entry = 3S~£ m|_s
Comments:
NOTE: Control liner and reagent blank weight data and balance check data are documented on other forms.
M5IPMRIX.WPD June 5, 1998 (rev. M17PMRI2.WPD July 29, 1999)
RCA#1 APPENDIX D
-------
PARTICULATE MATTER (FRONT-HALF) RINSES ANALYSIS DATA
MRI Project No. 104951.1.016.05.01
Client/Source: U.S. EPA OAQPS EMAD EMC / Cogentrix Unit 2A
Source Location: Rocky Mount, North Carolina
Sampling Location: Baghouse (Fabric Filter) Outlet Duct
Sampling Team Leader: Jim Surman Analyst: \^j-
Beaker Liner Size and Type: 250-mL Teflon® '/^
Acetone Lot No. BO 363
Sample Treatment: Acetone samples evaporated at ambient temperature and pressure in an
enclosure with HEPA-filtered air; then, desiccated and weighed to a constant weight.
Weight Unit: grams
Run No. •£
-------
PARTICULATE MATTER (FRONT-HALF) RINSES ANALYSIS DATA
MRI Project No. 104951.1.016.05.01
Client/Source: U.S. EPA OAQPS EMAD EMC / Cogentrix Unit 2A
Source Location: Rocky Mount, North Carolina
Sampling Location: Baghouse (Fabric Filter) Outlet Duct
Sampling Team Leader: Jim Surman Analyst:
Beaker Liner Size and Type: 250-mL Teflon® / ^
Acetone Lot No. BO 363
Sample Treatment: Acetone samples evaporated at ambient temperature and pressure in an
enclosure with HEPA-filtered air; then, desiccated and weighed to a constant weight.
Weight Unit: grams
Run No. SS? Beaker No. /J Sample No.
Sample Volume + Acetone Rinses of Bottle Beaker Liner + Sample Residue Weights
_ Gross Wt. Date Time
Beaker + Liner + Sample + Rinses Wt.
Beaker + Liner Tare Wt.
Sample + Rinses Wt.
Acetone Wt./0.79 = mLs Acetone:
Beaker Liner + Residue Gross Weight used for data entry:
Beaker Liner Tare Weight from Tare Weight Data:
Acetone Blank for data entry = Q_ mg/mL
Volume for data entry = ff-S^'y mLs
Comments:
Run No. *?£ Beaker No. /V Sample No.
Sample Volume + Acetone Rinses of Bottle Beaker Liner + Sample Residue Weiahts
M Gross Wt. Date Time
Beaker + Liner + Sample + Rinses Wt.
Beaker + Liner Tare Wt.
Sample + Rinses Wt.
Acetone Wt./0.79 = mLs Acetone:
Beaker Liner + Residue Gross Weight used for data entry:
Beaker Liner Tare WeigMtffom Tare Weight Data:
Acetone Blank for data entry = <2 mg/mL
Volume for data entry = 3 *J, ~7 mLs
Comments:
Run No. air? Beaker No. >/3 Sample No.
Sample Volume + Acetone Rinses of Bottle Beaker Liner + Sample Residue Weights
__ t Gross Wt. Date Time_
Beaker + Liner + Sample + Rinses Wt.
Beaker + Liner Tare Wt.
Sample + Rinses Wt.
Acetone Wt./0.79 = mLs Acetone:
Beaker Liner + Residue Gross Weight used for data entry: 3*'
Beaker Liner Tare Weight from Tare Weight Data:
Acetone Blank for data entry = C> mg/mL
Volume for data entry = <&£), "7 mLs
Comments:
NOTE: Control liner and reagent blank weight data and balance check data are documented on other forms.
M5IPMRIX.WPD June 5, 1998 (rev. M17PMRI2.WPD July 29, 1999)
RCA#1 APPENDIX D
-------
PARTICULATE MATTER (FRONT-HALF) RINSES ANALYSIS DATA
MR1 Project No. 104951.1.016.05.01
Client/Source: U.S. EPA OAQPS EMAD EMC / Cogentrix Unit 2A
Source Location: Rocky Mount, North Carolina
Sampling Location: Baghouse (Fabric Filter) Outlet Duct
Sampling Team Leader: Jim Surman Analyst:
Beaker Liner Size and Type: 250-mL Teflon®
Acetone Lot No. BO 363
Sample Treatment: Acetone samples evaporated at ambient temperature and pressure in an
enclosure with HEPA-filtered air; then, desiccated and weighed to a constant weight.
Weight Unit: grams
Run No. & & Beaker No. /& Sample No.
Sample Volume + Acetone Rinses of Bottle Beaker Liner + Sample Residue Weights
Gross Wt. Date Time
..<•«_
Beaker + Liner + Sample + Rinses Wt.
Beaker + Liner Tare Wt.
Sample + Rinses Wt.
Acetone Wt.70.79 = mLs Acetone:
Beaker Liner + Residue Gross Weight used for data entry:
Beaker Liner Tare Weight from Tare Weight Data:
Acetone Blank for data entry = ^ rng7mL
Volume for data entry = 3'}.~7 mLs
Comments:
Run No. 9/9 Beaker No. /"? Sample No.
Sample Volume + Acetone Rinses of Bottle Beaker Liner + Sample Residue Weights
Gross Wt. Date Time
* . *»*•* ^*.
Beaker + Liner + Sample + Rinses Wt.
Beaker + Liner Tare Wt.
Sample + Rinses Wt.
Acetone Wt./0.79 = mLs Acetone:
Beaker Liner + Residue Gross Weight used for data entry:
Beaker Liner Tare Weight from Tare Weight Data:
Acetone Blank for data entry = Q_ mg/mL
Volume for data entry = ^9.~? mLs
Comments:
Run No. J& Beaker No. So Sample No. ** _^»
Beaker + Liner + Sample + Rinses Wt.
Beaker + Liner Tare Wt. /J&'"3 3.>L
Sample + Rinses Wt.
Acetone Wt./0.79 = mLs Acetone:
Beaker Liner + Residue Gross Weight used for data entry:
Beaker Liner Tare Weight from Tare Weight Data:
Acetone Blank for data entry = Q mg/mL
Volume for data entry = ^fa-'J mLs
Comments:
NOTE: Control liner and reagent blank weight data and balance check data are documented on other forms.
M5IPMRIX.WPD June 5, 1998 (rev. M17PMRI2.WPD July 29. 1999)
RCA#1 APPENDIX D
-------
PARTICULATE MATTER (FRONT-HALF) RINSES ANALYSIS DATA
MRI Project No. 104951.1.016.05.01
Client/Source: U.S. EPA OAQPS EMAD EMC / Cogentrix Unit 2A
Source Location: Rocky Mount, North Carolina
Sampling Location: Baghouse (Fabric Filter) Outlet Duct
Sampling Team Leader: Jim Surman Analyst: .. /Cs
Beaker Liner Size and Type: 250-mL Teflon® /
Acetone Lot No. BO 363
Sample Treatment: Acetone samples evaporated at ambient temperature and pressure in an
enclosure with HEPA-filtered air; then, desiccated and weighed to a constant weight.
Weight Unit: grams
Run No. /PS* Beaker No. /7 Sample No.
Sample Volume + Acetone Rinses of Bottle Beaker Liner + Sample Residue Weights
Gross Wt. Date Time
Beaker + Liner + Sample + Rinses Wt. '^y-^. c?-"
Beaker + Liner Tare Wt. .
Sample + Rinses Wt.
Acetone Wt./0.79 = mLs Acetone: .
Beaker Liner + Residue Gross Weight used for data entry:
Beaker Liner Tare Weight from Tare Weight Data: g.b^S^r
Acetone Blank for data entry = O_ mg/mL
Volume for data entry = Sift "Z~- mLs
Comments:
Run No. J&& Beaker No. #& Sample No. S&/&3
Sample Volume + Acetone Rinses of Bottle Beaker Liner + Sample Residue Weights
Gross Wt. Date Time
,. A ft «*t
Beaker + Liner + Sample + Rinses Wt.
Beaker + Liner Tare Wt.
Sample + Rinses Wt.
Acetone Wt./0.79 = mLs Acetone:
Beaker Liner + Residue Gross Weight used for data entry:
Beaker Liner Tare Weight from Tare Weight Data:
Acetone Blank for data entry = O mg/mL
Volume for data entry = f£Z$'jJ mLs
Comments:
Run No. //& Beaker No. j«V Sample No.
Sample Volume + Acetone Rinses of Bottle Beaker Liner + Sample Residue Weights
Gross Wt. Date Time
._».— ***•
Beaker + Liner + Sample + Rinses Wt.
Beaker + Liner Tare Wt.
Sample + Rinses Wt.
Acetone Wt./0.79 = mLs Acetone:
Beaker Liner + Residue Gross Weight used for data entry:
Beaker Liner Tare Weight from Tare Weight Data:
Acetone Blank for data entry = O mg/mL
Volume for data entry = ^^"7 mLs
Comments:
NOTE: Control liner and reagent blank weight data and balance check data are documented on other forms.
MBIPMRIX.WPD June 5, 1998 (rev. M17PMRI2.WPD July 29. 19991
RCA#1 APPENDIX D
111 hi
-------
PARTICULATE MATTER (FRONT-HALF) RINSES ANALYSIS DATA
MRI Project No. 104951.1.016.05.01
Client/Source: U.S. EPA OAQPS EMAD EMC / Cogentrix Unit 2A
Source Location: Rocky Mount, North Carolina
Sampling Location: Baghouse (Fabric Filter) Outlet Duct
Sampling Team Leader: Jim Surman Analyst: ^/^,
Beaker Liner Size and Type: 250-mL Teflon® / &
Acetone Lot No. BO 363
Sample Treatment: Acetone samples evaporated at ambient temperature and pressure in an
enclosure with HEPA-filtered air; then, desiccated and weighed to a constant weight.
Weight Unit: grams
Run No. /' & Beaker No. «?<>£ Sample No.
Sample Volume + Acetone Rinses of Bottle Beaker Liner + Sample Residue Weiahts
Gross Wt. Date Time
Beaker + Liner + Sample + Rinses Wt. /S2?.te 3,&W~3 £>S-L
Beaker + Liner Tare Wt.
Sample + Rinses Wt.
Acetone Wt./0.79 = mLs Acetone: £ffi V
Beaker Liner + Residue Gross Weight used for data entry:
Beaker Liner Tare Weight from Tare Weight Data:
Acetone Blank for data entry = 0 mg/mL
Volume for data entry = J2&, V mLs
Comments:
Run No. / mg/mL
Volume for data entry = l!?Ps3 mLs
Comments:
Run No. SeS& Beaker No. ***r Sample No.
Sample Volume + Acetone Rinses of Bottle Beaker Liner + Sample Residue Weiahts
~, Gross Wt. Date Time
Beaker + Liner + Sample + Rinses Wt. /*%P&
Beaker + Liner Tare Wt. /V7.3
Sample + Rinses Wt.
Acetone Wt./0.79 = mLs Acetone:
Beaker Liner + Residue Gross Weight used for data entry:
Beaker Liner Tare Weight from Tare Weight Data:
Acetone Blank for data entry = O mg/mL
Volume for data entry = ^SV^C?7 mLs
Comments:
NOTE: Control liner and reagent blank weight data and balance check data are documented on other forms.
M5IPMRIX.WPD June 5. 1998 (rev. Ml 7PMRI2.WPD July 29. 19991
RCA#1 APPENDIX D
-------
PARTICULATE MATTER IN FILTER ASSEMBLY ANALYSIS DATA
MRI Project No. 104951.1.016.05.01
Client/Source: U.S. EPA OAQPS EMAD EMC / Cogentrix Unit 2A
Source Location: Rocky Mount, North Carolina
Sampling Location: Baghouse (Fabric Filter) Outlet Duct
t: -t'W???
Sampling Team Leader: Jim Surman
Analyst:
Filter Size and Type: 47mm diameter, Whatman 934-AH glass fiber filter
Filter Lot No. 29439A
Assembly Components: filter, aluminum foil gasket, and 316 stainless steel filter support
Filter Assembly Treatment: Heat at 105 °C for 3 hours, desiccate and weigh to a constant weight.
Weight Unit: grams
Run No.
Assembly No. /
Sample No.
Gross Wt.
Date
Time
Comments:
Assembly Gross Weight used for data entry: £7< 3'?"7/
Assembly Tare Weight from Tare Weight Data: J
Run No. J 13 Assembly No. & _ Sample No.
Gross Wt. Date Time Comments:
Assembly Gross Weight used for data entry:
Assembly Tare Weight from Tare Weight Data:
Run No.
Assembly No.
Gross Wt. Date
Sample No.
Time
Comments:
Assembly Gross Weight used for data entry:
Assembly Tare Weight from Tare Weight Data:
NOTE: Control and blank assembly weight data and balance check data are documented on other forms.
M5IPMFIX.WPD June 5, 1998 (rev. M17PMF12.WPD July 29, 1999!
RCA#1 APPENDIX D
-------
PARTICULATE MATTER IN FILTER ASSEMBLY ANALYSIS DATA
MRI Project No. 104951.1.016.05.01
Client/Source: U.S. EPA OAQPS EMAD EMC / Cogentrix Unit 2A
Source Location: Rocky Mount, North Carolina
Sampling Location: Baghouse (Fabric Filter) Outlet Duct
Sampling Team Leader: Jim Surman Analyst:
Filter Size and Type: 47mm diameter, Whatman 934-AH glass fiber filter
Filter Lot No. 29439A
Assembly Components: filter, aluminum foil gasket, and 316 stainless steel filter support
Filter Assembly Treatment: Heat at 105 °C for 3 hours, desiccate and weigh to a constant weight.
Weight Unit: grams
Run No. Assembly No. _ Sample No.
Gross Wt. Date Time Comments:
Assembly Gross Weight used for data entry: 3 *
Assembly Tare Weight from Tare Weight Data: J
Run No. c Assembly No. Sample No.
Gross Wt. Date Time Comments:
Assembly Gross Weight used for data entry:
Assembly Tare Weight from Tare Weight Data:
Run No. _ Assembly No. > _ Sample No.
Gross Wt. Date Time Comments:
Assembly Gross Weight used for data entry:
Assembly Tare Weight from Tare Weight Data:
NOTE: Control and blank assembly weight data and balance check data are documented on other forms.
j- M5IPMFIX.WPD June 5, 1998 (rev. M17PMFI2.WPD July 29, 1999)
RCA#1 APPENDIX D
-------
PARTICULATE MATTER IN FILTER ASSEMBLY ANALYSIS DATA
MRI Project No. 104951.1.016.05.01
Client/Source: U.S. EPA OAQPS EMAD EMC / Cogentrix Unit 2A
Source Location: Rocky Mount, North Carolina
Sampling Location: Baghouse (Fabric Filter) Outlet Duct
Sampling Team Leader: Jim Surman Analyst: Ss^/
Filter Size and Type: 47mm diameter, Whatman 934-AH glass fiber filter
Filter Lot No. 29439A
Assembly Components: filter, aluminum foil gasket, and 316 stainless steel filter support
Filter Assembly Treatment: Heat at 105 °C for 3 hours, desiccate and weigh to a constant weight.
Weight Unit: grams
Run No. 4/7 Assembly No. "7 Sample No.
Gross Wt. Date Time Comments:
Assembly Gross Weight used for data entry:
Assembly Tare Weight from Tare Weight Data:
Run No.
Assembly No. B Sample No.
Gross Wt. Date Time Comments:
Assembly Gross Weight used for data entry:
Assembly Tare Weight from Tare Weight Data:
Run No. J2P7 Assembly No. " Sample No.
Gross Wt. Date Time Comments:
Assembly Gross Weight used for data entry: 3 •• 2*4?'J»2--
Assembly Tare Weight from Tare Weight Data: <3* &£>*S&
NOTE: Control and blank assembly weight data and balance check data are documented on other forms.
M5IPMFIX.WPD June 5, 1998 (rev. M17PMFI2.WPD July 29, 1999)
11
RCA#1 APPENDIX D
-------
PARTICULATE MATTER IN FILTER ASSEMBLY ANALYSIS DATA
MRI Project No. 104951.1.016.05.01
Client/Source: U.S. EPA OAQPS EMAD EMC / Cogentrix Unit 2A
Source Location: Rocky Mount, North Carolina
Sampling Location: Baghouse (Fabric Filter) Outlet Duct
Sampling Team Leader: Jim Surman Analyst:
Filter Size and Type: 47mm diameter, Whatman 934-AH glass fiber filter
Filter Lot No. 29439A
Assembly Components: filter, aluminum foil gasket, and 316 stainless steel filter support
Filter Assembly Treatment: Heat at 105 °C for 3 hours, desiccate and weigh to a constant weight.
Weight Unit: grams
Run No. • Assembly No. Sample No.
Gross Wt. Date Time Comments:
3.
Assembly Gross Weight used for data entry:
Assembly Tare Weight from Tare Weight Data:
Run No. Assembly No. / _ Sample No.
Gross Wt. Date Time Comments:
3
Assembly Gross Weight used for data entry: •>•>
Assembly Tare Weight from Tare Weight Data: 3-'
Run No. £? & Assembly No. X^>< Sample No.
Gross Wt. Date Time Comments:
Assembly Gross Weight used for data entry:
Assembly Tare Weight from Tare Weight Data:
NOTE: Control and blank assembly weight data and balance check data are documented on other forms.
M5IPMRX.WPD June 5, 1998 (rev. Ml 7PMFI2.WPD July 29. 19991
12
RCA#1 APPENDIX D
-------
PARTICULATE MATTER IN FILTER ASSEMBLY ANALYSIS DATA
MRI Project No. 104951.1.016.05.01
Client/Source: U.S. EPA OAQPS EMAD EMC / Cogentrix Unit 2A
Source Location: Rocky Mount, North Carolina
Sampling Location: Baghouse (Fabric Filter) Outlet Duct
Sampling Team Leader: Jim Surman Analyst:
Filter Size and Type: 47mm diameter, Whatman 934-AH glass fiber filter
Filter Lot No. 29439A
Assembly Components: filter, aluminum foil gasket, and 316 stainless steel filter support
Filter Assembly Treatment: Heat at 105 °C for 3 hours, desiccate and weigh to a constant weight.
Weight Unit: grams
Run No. 7i Assembly No. /^ Sample No.
Gross Wt. Date Time Comments:
Assembly Gross Weight used for data entry: J
Assembly Tare Weight from Tare Weight Data:
Run No. "7 Assembly No. * Sample No.
Gross Wt. Date ' Time Comments:
Assembly Gross Weight used for data entry:
Assembly Tare Weight from Tare Weight Data:
Run No. " Assembly No. ^ Sample No.
Gross Wt. Date Time Comments:
Assembly Gross Weight used for data entry:
Assembly Tare Weight from Tare Weight Data:
NOTE: Control and blank assembly weight data and balance check data are documented on other forms.
M5IPMFIX.WPD June 5. 1998 (rev. M17PMFI2.WPD July 29. 1999]
RCA#1 APPENDIX D
-------
PARTICULATE MATTER IN FILTER ASSEMBLY ANALYSIS DATA
MRI Project No. 104951.1.016.05.01
Client/Source: U.S. EPA OAQPS EMAD EMC / Cogentrix Unit 2A
Source Location: Rocky Mount, North Carolina
Sampling Location: Baghouse (Fabric Filter) Outlet Duct
Sampling Team Leader: Jim Surman Analyst: _~
Filter Size and Type: 47mm diameter, Whatman 934-AH glass fijafsr fitter
Filter Lot No. 29439A
Assembly Components: filter, aluminum foil gasket, and 316 stainless steel filter support
Filter Assembly Treatment: Heat at 105 °C for 3 hours, desiccate and weigh to a constant weight.
Weight Unit: grams
Run No. Assembly No. Sample No.
Gross Wt. Date Time Comments:
Assembly Gross Weight used for data entry:
Assembly Tare Weight from Tare Weight Data:
Run No. *y>
Gross Wt. Date Time Comments:
3
Assembly Gross Weight used for data entry:
Assembly Tare Weight from Tare Weight Data:
NOTE: Control and blank assembly weight data and balance check data are documented on other forms.
.. . M51PMFIX.WPD June 5, 1998 (rev. M17PMFI2.WPD July 29, 1999)
RCA#1 APPENDIX D
-------
PARTICULATE MATTER IN FILTER ASSEMBLY ANALYSIS DATA
MRI Project No. 104951.1.016.05.01
Client/Source: U.S. EPA OAQPS EMAD EMC / Cogentrix Unit 2A
Source Location: Rocky Mount, North Carolina
Sampling Location: Baghouse (Fabric Filter) Outlet Duct
Sampling Team Leader: Jim Surman Analyst:
Filter Size and Type: 47mm diameter, Whatman 934-AH glass fiber niter
Filter Lot No. 29439A
Assembly Components: filter, aluminum foil gasket, and 316 stainless steel filter support
Filter Assembly Treatment: Heat at 105 °C for 3 hours, desiccate and weigh to a constant weight.
Weight Unit: grams
Run No. /&& Assembly No. /? Sample No.
Gross Wt. Date Time Comments:
Assembly Gross Weight used for data entry:
Assembly Tare Weight from Tare Weight Data:
Run No. JO Assembly No. & Sample No.
Gross Wt. Date Time Comments:
Assembly Gross Weight used for data entry:
Assembly Tare Weight from Tare Weight Data:
Run No. SJ& Assembly No. £? Sample No.
Gross Wt. Date Time Comments:
Assembly Gross Weight used for data entry:
Assembly Tare Weight from Tare Weight Data:
NOTE: Control and blank assembly weight data and balance check data are documented on other forms.
M5IPMFIX.WPD June 5, 1998 (rev. M17PMFI2.WPD July 29, 19991 .
RCA#1 APPENDIX D
-------
PARTICULATE MATTER IN FILTER ASSEMBLY ANALYSIS DATA
MRI Project No. 104951.1.016.05.01
Client/Source: U.S. EPA OAQPS EMAD EMC / Cogentrix Unit 2A
Source Location: Rocky Mount, North Carolina
Sampling Location: Baghouse (Fabric Filter) Outlet Duct
Sampling Team Leader: Jim Surman Analyst:
Filter Size and Type: 47mm diameter, Whatman 934-AH glass fibef fifter
Filter Lot No. 29439A
Assembly Components: filter, aluminum foil gasket, and 316 stainless steel filter support
Filter Assembly Treatment: Heat at 105 °C for 3 hours, desiccate and weigh to a constant weight.
Weight Unit: grams
Run No. > Assembly No. & Sample No.
Gross Wt. Date Time Comments:
Assembly Gross Weight used for data entry: &• *?73 d>
Assembly Tare Weight from Tare Weight Data: C
Run No. / Assembly No. &3 Sample No.
Gross Wt. Date Time Comments:
Assembly Gross Weight used for data entry: & --3
Assembly Tare Weight from Tare Weight Data: 3> '<
Run No. SJ Assembly No. 2? Sample No.
Gross Wt. Date Time Comments:
3.3-3X9 tf'3>-4?
Assembly Gross Weight used for data entry:
Assembly Tare Weight from Tare Weight Data:
NOTE: Control and blank assembly weight data and balance check data are documented on other forms.
* c M5IPMFIX.WPD June 5, 1998 (rev. M17PMFI2.WPD July 29. 19991
ID
RCA#1 APPENDIX D
-------
PARTICULATE MATTER CONTROLS ANALYSIS DATA
MRI Project No. 104951.1.016.05.01
Client/Source: U.S. EPA OAQPS EMAD EMC / Cogentrix Unit 2A
Source Location: Rocky Mount, North Carolina
Sampling Location: Baghouse (Fabric Filter) Outlet Duct
Sampling Team Leader: Jim Surman Analyst:
Balance: AND ER-120A, MRI #12007 / /
Weight Unit: grams
Control Filter Assembly Weights & Balance Checks:
Assembly No. #9 NIST Weight: Assembly No. && NIST Weight:
Original Tare Wt.: •£> •J&43 1 gram Original Tare Wt.: 3*3^3*} 1 gram
Current Wt. Date Time Balance Reading Current Wt. Date Time Balance Reading
3,3V3V
3.
oit -
Comments:
Control Beaker Liner Weights & Balance Checks:
Beaker No. #? NIST Weight: Beaker No. &° NIST Weight:
Original Tare Wt.: •&&%/& 1 gram Original Tare Wt.: &.* '?£2<37 1 gram
Current Wt. Date Time Balance Reading Current Wt. Date Time Balance Reading
3,
3.
/, #000
Comments:
Controls are filter assemblies and beaker liners selected from the original prepared lots that are used for sampling and analysis. They
are processed along with the assemblies and liners containing samples during analysis, i.e., they are heated, desiccated, and weighed
along with the assemblies and liners containing samples. The results are not used for correcting analytical data, but are useful in
monitoring changes between original tare weights and weights obtained during analysis of samples. Significant changes could
indicate problems in maintaining relatively constant environmental conditions in the laboratory, processing procedures not replicating
those used when tare weights were obtained, instrumentation calibration drift, and desiccant deterioration.
Each time filter assemblies or beaker liners are weighed, the balance is checked for accuracy by weighing NIST certified weights
approximating the weights of the assemblies or liners.
' I
M5IPMCOX.WPD June 5, 1998 (rev. M17PMC02.WPD July 29, 1999) 7 '
RCA#1 APPENDIX D
-------
PARTICULATE MATTER REAGENT BLANK ANALYSIS DATA
MRI Project No. 104951.1.016.05.01
Client/Source: U.S. EPA OAQPS EMAD EMC / Cogentrix Unit 2A
Source Location: Rocky Mount, North Carolina
Sampling Location: Baghouse (Fabric Filter) Outlet Duct
Sampling Team Leader: Jim Surman Analyst:
Beaker Liner Size and Type: 250-mL Teflon® / "
Acetone Lot No. BO 363
Sample Treatment: Acetone samples evaporated at ambient temperature and pressure in an
enclosure with HEPA-filtered air; then, desiccated and weighed to a constant weight.
Filter Size and Type: 47mm diameter, Whatman 934-AH glass fiber filter
Filter Lot No. 29439A
Assembly Components: filter, aluminum foil gasket, 316 stainless steel filter support
Filter Assembly Treatment: Heated at 105 °C for 3 hours, desiccated and weighed to a constant weight.
Weight Unit: grams
Acetone Blank Determination: For Run No.(s) 7-- : Beaker No. g* Sample No.
Acetone Reagent Blank Sample Volume ' . Beaker Liner + Sample Residue Weights
_ Gross Wt. Date Time
Beaker + Liner + Acetone Sample Wt.
Beaker + Liner Tare Wt. /&&*
Acetone Sample Wt.
A. Acetone Wt./0.79 = mLs Acetone:
Beaker Liner + Residue Gross Weight used for Wank determination:
Beaker Liner Tare Weight from Tare Weight Data:
B. Net Weight of Residue in beaker liner: ^
Acetone Blank (B x 1000/A) for data entry: O mg/mL
Comments:
Filter Assembly Blank Determination: For Run No.(s) /?£-l— Assembly No. &o Sample No. /i& "7
Gross Wt. Date Time Comments:
3.
A. Assembly Gross Weight used for blank determination: 3,
B. Assembly Tare Weight from Tare Weight Data: J^
Net Assembly Weight Difference (A - B) for data entry: O_
[retain minus sign if value is negative]
NOTE: Control liner and filter assembly weights and balance check data are documented on another form.
M5IPMBLX.WPD June 5, 1998 (rev. M17PMBL2.WPD July 29, 19991
18
RCA#1 APPENDIX D
-------
BEAKER LINER TARE WEIGHT DATA
MRI Project No. 104951.1.016.05.01
Sampling Team Leader: Jim Surman
Beaker Liner Size and Type: 250-mL Teflon®
Analyst:
Beaker Liner Treatment: Wash to clean, rinse with Dl water, dry at 105 °C, insert into glass beakers previously
cleaned in the same manner, desiccate for 24 hours, and weigh to a constant.
Weight Unit: grams
Date:
Time Started:
Beaker Liner in
Beaker I.D. No.
/'J
#0
Balance Check before beaker liners are weighed:
Balance Used:
Weight Value:
Balance Reads:
A0DOD
First Weiahina
Second Weiahina
Third Weiahina
Average Weight
or Weight to be
Used as the Tare
3,
3
3. -
&23J3
Balance Check after beaker liners are weighed:
Balance Reads: "~
COMMENTS:
3.
3.
&
. 73&ZL.
M5IBEAKX.WPD June 4, 1998 (rew. M17BEAK2.WPD July 29, 19991
RCA#1 APPENDIX D
19
-------
BEAKER LINER TARE WEIGHT DATA
MRI Project No. 104951.1.016.05.01
Sampling Team Leader: Jim Surman Analyst: '/
f &
Beaker Liner Size and Type: 250-mL Teflon®
Beaker Liner Treatment: Wash to clean, rinse with Dl water, dry at 105 °C, insert into glass beakers previously
cleaned in the same manner, desiccate for 24 hours, and weigh to a constant.
Weight Unit: grams
Date:
Time Started:
Balance Check before beaker liners are weighed:
Balance Used:
Weight Value:
Balance Reads:
Average Weight
Beaker Liner in or Weight to be
Beaker I.D. No. First Weighing Second Weighing Third Weighing Used as the Tare
*? *7^"?"~7 ^7 ^?-^"C? "*7 ~"Z> ~J o ~^? "*7
^X.1 X^<** ij S t*^-> S &f \JL * \J-f ^ **< *^ ^
Balance Check after beaker liners are weighed:
Balance Reads:
COMMENTS:
M5IBEAKX.WPD June 4, 1998 (rev. M17BEAK2.WPD July 29, 19991
20
RCA#1 APPENDIX D
-------
FILTER ASSEMBLY TARE WEIGHT DATA
MRI Project No. 104951.1.016.05.01
Sampling Team Leader: Jim Surman
Analyst:
Filter Size and Type: 47mm diameter, Whatman 934-AH glass fiber filter
Filter Lot No. 29439A /Z-fV^
Assembly Components: filter, aluminum foil gasket, and 316 stainless steel filter support
Filter Assembly Treatment: Heat at 105 °C for 3 hours, desiccate, and weigh to a constant weight.
Weight Unit: grams
Date: $'
, Time Started:
Balance Check before filter assembles are weighed:
Balance Used:
i!
10
n
n
rf
tf
n
it
Weight Value: /b, OQOo
Balance Reads: '
Assembly No.
'•jf &
-------
FILTER ASSEMBLY TARE WEIGHT DATA
MRI Project No. 104951.1.016.05.01
Sampling Team Leader: Jim Surman Analyst: (^
Filter Size and Type: 47mm diameter, Whatman 934-AH glass fiber filter
Filter Lot No. 29439A
Assembly Components: filter, aluminum foil gasket, and 316 stainless steel filter support
Filter Assembly Treatment: Heat at 105 °C for 3 hours, desiccate, and weigh to a constant weight.
Weight Unit: grams
Date: a'i'1,1
;,Time Started: /"? (6 /
Baiance Check after fiiter assemblies are weighed:
Balance Reads: ^
COMMENTS:
22''15"':|u:)<-''vprj •'•••"•'-4. !9S" ":-..• M17FILT2.WPU July 29. 19991
RCA#1 APPENDIX D
-------
40 CFR 60, APPENDIX A, METHOD 17 - PARTICULATE MATTER TRAIN (M17)
FIELD REAGENT BLANK PREPARATION DATA
MRI Project No. 104951.1.016.05.01
Client/Source: U.S. EPA OAQPS EMAD EMC / Cogentrix Unit 2A
Source Location: Rocky Mount, North Carolina
Sampling Location: Baghouse (Fabric Filter) Outlet Duct
Blank(s) Prepared By: tSSZtt^Trvfr?— Date:
Weights below are in grams.
Sample Bottle Tare Bottle Gross Net Sample
Reagent Blank Description Number Weight Weight Weight
Acetone for particulate matter
Volume needed: 100 mLs
Lot Number: BO 363 /105
Filter Assembly for particulate matter
Type: Whatman 934-AH
Filter Assembly Number: _
Filter Lot Number: 29439A / 107
NOTE: Lots may be identified above by a manufacturer's fot number or by the date of reagent preparation. If different lots of
a particular reagent are used, indicate the applicable test and/or run number(s) and sampling location(s) where the train(s)
loaded and/or recovered with that reagent are used (i.e., list each reagent blank sample number with the applicable test
and/or run number(s) and sampling location^} below}.
Sample Number(s) For Test and/or Run Numberfs) For Sampling Location(s)
COMMENTS:
M17D8LK.WPD May 13, 1999 (rev. M17DBLK2.WPD July 29, 1999)
23
RCA#1 APPENDIX D •
-------
RCA #1 Appendix E
M17 Post-Test Calibration Sheets
MR]-OPPT\R4703-0:-07 Appendices Covers.WPD
-------
ON SITE MERCURY BAROMETER READING CORRECTION
AND ANEROID BAROMETER CALIBRATION CHECK AT TEST LOCATION
Mercury Barometer Description: Princo Mode! 453, S/N W13559
Mercury Barometer Location: Rant Control Room
Distance Of Barometer From Test Site: 0.00 miles
Altitude Of Barometer Above Sea Level: 124.0 feet
Latitude (north): 36 degrees, 0.00 minutes
Facility: Cogentrix of Rocky Mount, North Carolina
Test Site And Sampling Location: Unit 2A Baghouse Outlet Duct
MRI Project No. 104951.1.016.05.01
Date: 08/31/99
Time: 1051
Readings Obtained By: J. Surman
Observed Barometer Reading: 30.13 in. Hg
Mercury Column Temperature: 73 "F
Correction For Temperature: -0.12 in. Hg
Reading Corrected For Temperature: 30.01 in. Hg
Correction For Gravity: -0.03 in. Hg
Temperature Corrected Reading Corrected For Gravity: 29.98 in. Hg
Aneroid Barometer I.D. No.: Y-2101
Reading Before Adjustment: 29.97 in. Hg
Calibration Check Result: within 0.1 in. Hg
Reading After Adjustment:
-------
METHOD 5 METERING CONSOLE CALIBRATION
CRITICAL ORIFICE BRACKETING DATA
MRI Project No.
Date:
Operator
Metering Console No.
Dry Gas Meter Factor (Y):
Orifice Used for the Calibration:
Ambient Temperature Meter No.
104951. 1.016.05.C
08/31/99
D. Neal
N11
1.010
D19
Y-0815
Note: Critical orifice coefficients are in English units.
Critical Orifice Being Evaluated
Critical Orifice No.
D19
Critical Orifices Used For Bracketing
First Orifice
Critical Orifice No.
Coefficient (K1):
Second Orifice
Critical Orifice No.
Coefficient (K1):
D16
0.44410
D24
0.65490
CALIBRATION GAS VOLUME DATA
Initial Dry Gas Meter Gas Volume, ft.3
Final Dry Gas Meter Gas Volume, ft.3
Net Dry Gas Meter Gas Volume (Vm), ft.3
First Orifice
814.898
5.796
Second Orifice
815.202
823.799
"8.597
CALIBRATION CONDITIONS DATA
Dry Gas Meter Temperature, °F:
Initial Inlet Temperature, °F
Final Inlet Temperature, °F
Initial Outlet Temperature, °F
Final Outlet Temperature, °F
Average Dry Gas Meter Temperature (tm), °F
Time, seconds
Orifice Meter Delta-H, inches w.c.
Barometric Pressure, in. Hg
Critical Orifice Inlet (Ambient) Temperature, *F:
Initial Ambient Temperature, °F
Final Ambient Temperature, "F
Average Critical Orifice Inlet Temperature (tamb), °F
Pump Vacuum, in. Hg
78.0
81.0
80.0
75.0
82.0.
"77.0
76.0
78.0
77.3
600
_79.5
600"
1.100
2.450
29.95
71.4
29.95
72.2
72.2
72.2
_7t.8_
18
72.2
18
COMPUTED CALIBRATION RESULTS
Critical Orifice Gas Volume (Vcr (std)), std. ft.3
Dry Gas Meter Gas Volume (Vm (std)), std. ft.3
Factor (Y) Obtained With Bracketing Orifice
5.770
8.505
5.717
8.472
1.009
1.004
CRITICAL ORIFICE ACCEPTABILITY
Criterion: All Ys Must Be Within 2% Of All Other Ys
Larger % Difference Between Dry Gas Meter Factor (Y)
And Factor (Y) Obtained With The Bracketing Orifice
Larger % Difference Between Factors (Ys)
Obtained With Bracketing Orifices
Acceptability Result
0.08%
0.61%
All Orifices Are Acceptable
Remarks:
CRORBRKT.WK4 10/24/96 (rev. 4951 BRKT.WK4 08/31/99 10:31 AM)
RCA#1 APPENDIX E
-------
METHOD 5 METERING CONSOLE CALIBRATION WITH CRITICAL ORIFICE
MRI Project No.
Date:
Operator:
104951. 1.016.05.C
8/31/99
D. Neal
1 Metering Console No.
Previous Dry Gas Meter Factor (Y):
Calibrated Critical Orifice No.
Critical Orifice Coefficient in English Units (K):
| Ambient Temperature Meter No.
N10
1.019
D19
0.51210
Y-0815
CALIBRATION GAS VOLUME DATA
Initial Dry Gas Meter Gas Volume, ft.3
Final Dry Gas Meter Gas Volume, ft.3
Net Dry Gas Meter Gas Volume (Vm), ft.3
CALIBRATION CONDITIONS DATA
Dry Gas Meter Temperature, °F:
Initial Inlet Temperature, "F
Final Inlet Temperature, °F
Initial Outlet Temperature, °F
Final Outlet Temperature, °F
Average Dry Gas Meter Temperature (tm), °F
Time, seconds
Orifice Meter Delta-H, inches w.c.
Barometric Pressure, in. Hg
Critical Orifice Inlet (Ambient) Temperature, °F:
Initial Ambient Temperature, °F
Final Ambient Temperature, "F
Avg. Critical Orifice Inlet Temperature (tamb), °F
Pump Vacuum, in. Hg
COMPUTED CALIBRATION RESULTS
Critical Orifice Gas Volume (Vcr (std)), std. ft.3
Dry Gas Meter Gas Volume (Vm (std)), std. ft.3
Dry Gas Meter Calibration Factor (Y)
Orifice Meter Delta-H@
AVERAGE CALIBRATION RESULTS
Average Dry Gas Meter Calibration Factor (Y)
Average Orifice Meter Delta-H@
CALIBRATION RESULTS COMPARISON
Criterion: Y Must Be Within 2% Of Average Y
Percent Difference Of Y From Average Y
Tolerance Result
COMPARISON WITH PRETEST RESULTS
Criterion: Y Must Be Within 5% Of Previous Y
% Difference Of Average Y From Previous Y
Tolerance Result
Run 1
V'i ,V^' ^
494.699
501.362
6.663
72.0
73.0
70.0
71.0
71.5
600
1.450
29.95
•qs^Gfr-pff •*• ••••jg^a-r^ rv •** "-TV
*„.,*.*, ' *>? A *, &
672
68.0
67.6
18
; *i- ' V*»
6.679
6.649
1.005
1.831
fv* . .'•* Ogft. \Mri
.**."*,«*& I***.. '. .£ *fthMt> ki*«&k
1.007
1.828
> r '"* " ,~v
» f 4 *
ife* > ** « Jk A
0.26%
PASS
SM'"iSMf^0i€
'K''tf-' <'$tAb! fe "J: ' W£ '"m
rtc,^-y ^fi5,-."^4.%*y^j;^i',^
ii&Si^mS&^S
1.16%
PASS
Run 2
"'•'''"y't'^m-'^,"'^' ' '
***&£**'&•.,•&
501.362
508.022
6.660
**" ' 74.0
76.0
71.0
71.0
73.0
600
1.450
29.95
—i- * «n ^p?!7W:raf.^j$r'-'""1^r vwsr~*;
«.' ^jVJ««. ~, '!
686
68.4
68.5
18
* 'V ">' " "
** , r m ^ ,- \
6.674
6.627
1.007
1.829
Run3
' "*x* fi*'1,* * >?i "
( f~Ja£ AI J-« « i J
508.022
514.681
6.659
77.0
78.0
72.0
72.0
74.8
600
1.450
29.95
3*5*?3^3&*!I,uj
688
69.2
69.0
18
.^Wt-X^'i"1^
6.671
6.605
1.010
1.825
' "' *«•* ?***•
*^ j/C^-.- /''
* 0.02% *°^
PASS
9 ' -••rsf-^'ii--- - •.
{ ^A,*-/*
» ., " ffe^ ;
; JLU v ?j«a *~ * * <
0.28%
PASS
Y = 1 .0071 70458786064
Remarks:
CRORCALB.WK4 10/24/96 (rev. 4951016.WK4 08/31/99 10:21 AM)
RCA#1 APPENDIX E
-------
CONSOLE CALIBRATION WORKSHEET
Job No. /0e/?£/./.0/6.0S'.0/ Console No.
Date 8'3l~?(} Orifice No.
Performed By < v&eL _ K Factor
Barometer > $ in. Hg. Previous Y /< O •' J
NOTE: Prior to running calibration, connect mercury manometer
to sample orifice. Turn on pump and bring mercury manometer up
to 18.0 in. Hg. Record mercury manometer and console vacuum
gauge readings below. Insert critical orifice into console
sample orifice. Set console vacuum gauge at 18.0 in. Hg. +/-
the console vacuum gauge correction factor calculated below.
Mercury manometer readings: ^//f + s^/fl - 18.0 In. Hg.
Console vacuum gauge reading: In. Hg.
Console vacuum gauge correction factor: ~Jj?^J In, Hg.
/&< o OfJ S^l-fl cf
r £X
RUN #1 RUN #2 RUN #3
DGM Initial Volume:
Initial: ?7Y.6/f 3~e/.j(,'L* S'oS.p'J-L
Final:
DGM Inlet Temperature:
Initial: 7> ?7 7*7
Final :
73 1£ 73
DGM Outlet Temperature:
Initial: 7^ 7/ 7>
•^l I —-» /
Final: // //
Time of run ( In Seconds ) : £ff° £°° 6°°
Orifice Delta H (in. H20) : A Y>
Room Temperature:
Initial
18.
Final: 6&-D
Pump Vacuum (in. Hg ): 18 . 0 18 . 0 18.0
Calibration Records\Calibration Forms\concalws4d.doc Revised 02/03/99
RCA#1 APPENDIX E
-------
M5 CONSOLE POST TEST CHECKLIST
Job No .
, A 0*it of.
Date
Console No.
Performed By
Place a check (in black ink) in the space provided after the
required checks are performed.
1. \ Perform positive leak check of Delta H manometer.
(See back of this sheet.)
2. \/ Leak check Delta P manometer.
3. X/4 Clean pump.
4. y Clean muffler jar(s).
Inspect/refill oiler jar.
\
6. \ Calibrate DGM thermocouples:
Note : Reading must be
Within +/-5. 4°F
DGM Inlet :
DGM Outlet:
Reference
Thermometer*
°F
61 Y
69-2-
DGM
Thermocouple
°F
6'?
7. X Digital clock/timer in place and functional.
\ Vacuum check. (Leak check at 25 in. Hg . vacuum. Leak
rate should be zero.)
Check indicator lights.
Check thermocouple switched.
Check fan.
Check pump heater.
Check heat controllers.
Check Orsat pump and rotameter.
If any of the above items were replaced or repaired, please
document that information below:
9.
10 .
11.
12 .
13 .
14.
X
X
\
X
\
\-
* Reference Thermometer: 4J7m &3f Serial Number:
Calibration Records\Calibration Forms\M5check-doc
Revised 10/28/98
RCA#1 APPENDIX E
-------
Procedure for positive leak check Delta H manometer:
1. Pump must not be run prior to this test. Pump needs to be
cool in order to get an accurate reading.
2. Pump pressure and vacuum lines must be connected to console.
3. Null switch on console must be in the down position so
solenoid valve is open to the sampling stream as it is
during testing.
4. Plug meter exhaust and clamp off bottom tube from exhaust
which goes to the Orsat pump.
5. Plug sample orifice.
6. Close main flow control valve.
7. Open fine control valve.
8. Disconnect right side Delta H manometer tube on front of
console.
9. Blow into tubing until manometer reads 5 to 7 inches of
water, and clamp off.
There should be no change in manometer reading.
10 . Make certain you remove plug and clamp from meter exhaust
immediately after this test to avoid damage to the meter
pump when pump is started UD!
caiibrec\m5check 03/09/98
RCA#1 APPENDIX E
-------
METHOD 5 METERING CONSOLE CALIBRATION WITH CRITICAL ORIFICE
MRI Project No.
Date:
Operator
104951. 1.016.05.C
8/31/99
D. Neal
1 Metering Console No,
Previous Dry Gas Meter Factor (Y):
Calibrated Critical Orifice No.
Critical Orifice Coefficient in English Units (K1):
Ambient Temperature Meter No.
N11
1.023
D19
0.51210
Y-0815
CALIBRATION GAS VOLUME DATA
Initial Dry Gas Meter Gas Volume, ft.3
Final Dry Gas Meter Gas Volume, ft.3
Net Dry Gas Meter Gas Volume (Vm), ft.3
CALIBRATION CONDITIONS DATA
Dry Gas Meter Temperature, °F:
Initial Inlet Temperature, °F
Final Inlet Temperature, °F
Initial Outlet Temperature, °F
Final Outlet Temperature, °F
Average Dry Gas Meter Temperature (tm), °F
Time, seconds
Orifice Meter Delta-H, inches w.c.
Barometric Pressure, in. Hg
Critical Orifice Inlet (Ambient) Temperature, °F:
Initial Ambient Temperature, °F
Final Ambient Temperature, °F
Avg. Critical Orifice Inlet Temperature (tamb), °F
Pump Vacuum, in. Hg
COMPUTED CALIBRATION RESULTS
Critical Orifice Gas Volume (Vcr (std)), std. ft.3
Dry Gas Meter Gas Volume (Vm (std)), std. ft.3
Dry Gas Meter Calibration Factor (Y)
Orifice Meter Delta-H@
AVERAGE CALIBRATION RESULTS
Average Dry Gas Meter Calibration Factor (Y)
Average Orifice Meter Delta-H @
CALIBRATION RESULTS COMPARISON
Criterion: Y Must Be Within 2% Of Average Y
Percent Difference Of Y From Average Y
Tolerance Result
COMPARISON WITH PRETEST RESULTS
Criterion: Y Must Be Within 5% Of Previous Y
% Difference Of Average Y From Previous Y
Tolerance Result
V = 1.01 0024834051 550
Run 1
: , ^
: **\ M « ^.^
788.802
795.416
6.614
72.0
74.0
71.0
72.0
72.3
600
1.500
29.95
70.0
70.8
70.4
18
Vj * -^, ',' '
>K A * #~ •*«;•
6.662
6.592
1.011
1.902
,r.,,,,,, .,,,.,„ ., ,„. -. -T.¥.,_;
v 1 •» , »ljt edswt> '
1.010
1.898
%: *' tu ~*.
a* ajfe \ ^V|*£»
0.06%
PASS
U-~ - i^rf^r
•*<•<•* >*?*».
,> ,. * . > w * •
/ & d * i t Tvutt «»
1.27%
PASS
Run 2
#v ts^^r 3
>\ i * ^ -f«,%g" i _• »*y
795.416
802.042
6.626
ISvMV^l
74.0
76.0
72.0
73.0
73.8
600
1.500
29.95
**"*7l'.2*"fc' '*"
71.0
71.1
18
/!f-'>'.-«••' " "' 'KS
^.i**^":,,** j
802.042
808.703
6.661
'•i «,^i ;"vV'lr^ ^
'«^ t*-» t«*^ • *
^,r*a.,4,V\i5&»&
770
78.0
73.0
74.0
75.5
600
1.500
29.95
,, , •7Y6- -
71.6
71.6
18
k5 ! '* "-^
6.654
6.598
1.008
1.895
::,-^ :y tfc"i
-woSt •*" / * *•
0.1 5%"
PASS
Remarks:
CRORCALB.WK4 10/24/96 (rev. 4951016.WK4 08/31/99 10:40 AM)
RCA#1 APPE>JDIX E
-------
CONSOLE CALIBRATION WORKSHEET
Job No. /0) Console No.
Date S"3i~ 99 Orifice No. £)//
Performed By tO< Wdfo^ K Factor Q- 5/^
Barometer /•/'-'5* in. Hg . Previous Y A_
NOTE : Prior to running calibration, connect mercury manometer
to sample orifice. Turn on pump and bring mercury manometer up
to 18.0 in. Hg . Record mercury manometer and console vacuum
gauge readings below. Insert critical orifice into console
sample orifice. Set console vacuum gauge at 18.0 in. Hg . +/-
the console vacuum gauge correction factor calculated below.
Mercury manometer readings: sJfa + A///P = 18 . 0 In. Hg.
Console vacuum gauge reading: - ""^ In. Hg .
Console vacuum gauge correction factor: //- & In. Hg .
RUN #1 RUN #2 RUN #3
DGM Initial Volume: ,, _ , , A^
Initial: 738.8°?- 7 73
Time of run ( In Seconds ) : ^
-------
CONSOLE BRACKETING WORKSHEET
Job No. /O /1 Bracketing Orifice No . 2
New Y Factor /, QtQ _ K Factor
Barometer j-9 . f j" in. Hg .
NOTE : Prior to running calibration, connect mercury manometer
to sample orifice. Turn on pump and bring mercury manometer up
to 18.0 in. Hg . Record mercury manometer and console vacuum
gauge readings below. Insert critical orifice into console
sample orifice. Set console vacuum gauge at 18.0 in. Hg . +/-
the console vacuum gauge correction factor calculated below.
Mercury manometer readings: //* + f^j = 18.0 in. Hg .
Console vacuum gauge reading: - • — in. Hg.
Console vacuum gauge correction factor: /o- ° in. Hg .
RUN #1 RUN #2
DGM Initial Volume: . _ _
Initial: &» 1. 101-
Final: 8 / V . 8 18 8^3 . 7 f 7
DGM Inlet Temperature: _.
Initial: iff 9*
Final:
DGM Outlet Temperature:
Initial: 7j" 77
Final:
Time of run ( In Seconds ):
Orifice Delta H(in. H20) : /.
Room Temperature:
initial: 7A
Final
Pump Vacuum (in. Hg ): _ 18 . 0 _ _ 18 . 0 _
Calibration RecordsNCalibration Forms\eonbrkws4d.doc Revised 02/03/99
RCA#1 APPENDIX E
-------
M5 CONSOLE POST TEST CHECKLIST
Job No.
. /• Qf 6-
Date
Console No.
Performed By
Place a check (in black ink) in the space provided after the
required checks are performed.
1. v Perform positive leak check of Delta H manometer.
(See back of this sheet.)
2
3
4
5
\
V
Leak check Delta P manometer.
Clean pump.
Clean muffler jar(s).
Inspect/refill oiler jar.
6. \ Calibrate DGM thermocouples:
Note : Reading must be
Within +/-5.4°F
DGM Inlet:
DGM Outlet:
Reference
Thermometer*
°F
6?.r
6?.1
DGM
Thermocouple
°F
Digital clock/timer in place and functional.
Vacuum check. (Leak check at 25 in. Hg . vacuum. Leak
rate should be zero.)
Check indicator lights.
Check thermocouple switched.
Check fan.
Check pump heater.
Check heat controllers.
Check Orsat pump and rotameter.
If any of the above items were replaced or repaired, please
document that information below:
7.
8.
9 .
10.
11 .
12 .
13.
14.
X
V
N/
\
X
>v/
Vy
^
* Reference Thermometer:
Serial Number:
Calibration Records\Calibration Forms\M5check-doc
Revised 10/28/98
10
RCA#1 APPENDIX E
-------
Procedure for positive 1eak cherk Delta H manometer:
I. Pump must not be run prior to this test. Pump needs to be
cool in order to get an accurate reading.
2. Pump pressure and vacuum lines must be connected to console.
3. Null switch on console must be in the down position so
solenoid valve is open to the sampling stream as it is
during testing.
4. Plug meter exhaust and clamp off bottom tube from exhaust
which goes to the Orsat pump.
5. Plug sample orifice.
6. Close main flow control valve.
7. Open fine control valve.
8. Disconnect right side Delta H manometer tube on front of
console.
9. Blow into tubing until manometer reads 5 to 7 inches of
water, and clamp off.
There should be no change in manometer reading.
10 . Make certain you remove plug and clamp from meter exhaust
immediately after this test to avoid damage to the meter
pump when pump is started UP!
calibrec\m5check 03/09/98
11
RCA#1 APPENDIX E
-------
GOOSENECK THERMOCOUPLE CALIBRATION DATA FORM
Job No. /£>Vf> /, //1>/( ,o$~.
-------
GOOSENECK THERMQCniTPT.F CALIBRATION DATA FORM
Job No.
Date
' /•
Pyrometer No.
Performed By
Reference Thermometer
Serial Number
Calibration Method: Direct comparison of gooseneck thermocouple
with reference thermometer in ambient air.
Goose-neck
T.C. No.
u/t->
UH-3)-
Leak Check & Check
Valve Pass/No-pass
fas
fas
Ref. Thermometer
Temperature (*F)
7o. /
"7 o.o
Pyrometer Temp.
(*F)
7/
7o
Temp. Difference
+/-2T
-co.7
0
Calibration Records\CaIibration Forms\GntccaLdoc
Revised 10/28/98
RCA#1 APPENDIX E
13
-------
STACK THERMOCOUPLE CALIBRATION DATA FORM
Job No.
Date
f • I •
Stack Thermocouple No.
Probe No. /?
Performed By
Avg. Stack Temp. (°F) /8S
Pyrometer No.
Reference Instrument: Hart Scientific Model No. 9100A, Serial
No. 84414 Dry-well, HDRC Handheld Block A. This instrument
is calibrated in accordance with ITS-90 and ANSI/NCSL Z540-1
Reference Instrument
Temp. ("F)
6jr-5"^/m
(
o
Temp. Difference
(%)
0.3!")-
-0.181-
0
;ref. Temp., F + 460) - (pyro. Temp., F + 460)
(ref. Temp., F + 460)
X 100 < 1.5%
Calibration RecordsVCalibration FormsVSTCHartdoc
Revised 10/29/98
14
RCA#1 APPENDIX E
-------
STACK THERMOCOUPLE CALIBRATION DATA FORM
Job No. /os/ff/, /•&.'(>, OS'01 Stack Thermocouple No.
Date ff'3'-?9 Probe No. £
Performed By
Pyrometer No.
Avg. Stack Temp. (°F)
Reference Instrument: Hart Scientific Model No. 9100A, Serial
No. 84414 Dry-well, HDRC Handheld Block A. This instrument
is calibrated in accordance with ITS-90 and ANSI/NCSL Z540-1
Reference Instrument
Temp. (T)
Pyrometer Temp.
(•F)
Temp. Difference
(*F)
Temp. Difference
;ref. Temp., F + 460) - (pyro. Temp., F + 460
(ref, Temp., F + 460)
X 100 < 1.5%
Calibration Records\Calibration Forms\STCHartd»c
Revised 10/29/98
RCA#1 APPENDIX E
15
-------
Type S Pitot Tube Inspection Data Form
Pitot Tube #:
Probe #: A
Date:
Job#:
Pitot tube assembly level?
Pitot tube openings damaged?
«, - 0 °
Pi - 2- °
Performed By:
Yes
Yes (explain below)
A =
Y = 0 °, 6 = ^_
z = A sin Y 0_
a) = A sin 9 0*0 fy (in); (< 0.03125 in)
(in)
(in), PB =
(in), DT =
Calibration required?
Comments:
Yes
No
No
No
(in)
16
1*11*8
-------
Type S Pitot Tube Inspection Data Form
Pitot Tube #:
Probe #:
Date:
Job#:
Performed By:
Pitot tube assembly level?
Pitot tube openings damaged?
Yes
Yes (explain below)
Comments:
No
No
Pi = ° (<5°),
z = A sin Y O
o) = Asin6 0*0(1
PA= ^^ (in)>
Calibration required?
(32 = ( (<5 ,
/ °, A = frl^
(in); (< 0.125 in)
(in); (< 0.03 125 in)
PB = 6/YlC (in),
Yes ^^ No
I
(in)
DT = tfSLfo
(in)
"0 AorB ~V _J~
0.48 CM < Dt < 0.95 CM
(3/16 in.) (3/8 in.)
Transverse
Tube Axis
Transverse
Tube Axis
Calibration Records\Calibration Forms\newpitot.doc
RCA#1 APPENDIX E
01/18/99
17
-------
RCA#1 Appendix F
PM CEMS Data for Each Run
MRJ-OPPT\R4703-02-07 Appendices Covers WPD
-------
RCA #1 Testing - Run 1
8/26/99 ESC P5B
Time raw mA
15:44
15:45
15:46
15:47
15:48
15:49
15:50
15:51
15:52
15:53
15:54
15:55
15:56
15:57
15:58
15:59
16:00
16:01
16:02
16:03
16:04
16:05
16:06
16:07
16:08
16:09
16:10
16:11
16:12
16:13
16:14
16:15
16:16
16:17
16:18
16:19
16:20
16:21
16:22
16:23
16:24
16:25
16:26
16:27
16:28
16:29
16:30
16:31
16:32
17.86
15.20
12.69
12.30
13.05
13.38
14.00
14.63
13.68
14.48
14.88
14.38
13.95
14.07
14.80
12.38
12.66
14.43
14.51
16.95
18.45
16.82
12.21
12.78
13.62
13.24
14.32
14.87
14.51
15.40
15.62
15.70
14.65
14.94
15.62
14.20
12.39
14.33
15.09
17.10
19.03
19.31
13.88
13.11
14.09
13.71
14.90
15.64
15.88
I : High PM concentration
Durag 300-40 Durag F904K Moisture
raw ra mA raw mA %
25.75
24.01
30.67
30.58
29.95
23.74
24.82
25.66
24.25
24.88
25.90
25.66
23.71
25.45
27.73
35.11
40.03
39.82
29.74
27.10
27.58
27.34
28.15
30.22
33.22
24.85
26.44
26.26
26.71
26.71
27.67
28.15
24.46
26.08
27.82
33.79
43.12
39.91
36.64
27.73
28.06
31.12
29.62
34.27
36.13
30.61
27.19
28.60
29.92
13.68
13.68
13.68
13.68
13.68
13.68
13.68
13.68
13.68
13.68
13.68
13.68
13.96
14.81
14.81
14.80
14.80
14.80
14.81
14.80
14.80
14.80
14.80
14.80
14.80
14.74
14.56
14.56
14.56
14.56
14.56
14.56
14.56
14.56
14.56
14.56
14.56
14.56
14.89
14.89
14.77
14.77
14.77
14.83
14.93
14.93
14.93
15.17
15.17
14.93
15.05
15.17
15.17
15.17
15.17
15.17
15.17
15.17
15.05
15.17
14.93
14.93
14.93
14.93
15.05
15.17
14.93
14.93
15.05
14.93
14.57
14.93
15.05
15.05
15.05
14.93
14.93
14.93
14.93
15.05
14.95
14.93
15.00
14.89
15.01
14.89
14.89
Temp.
deg C
86
86
86
86
86
85
84
84
84
84
84
84
84
84
84
84
84
84
84
84
84
84
84
84
84
84
84
84
84
84
84
84
84
84
84
84
84
84
84
84
84
84
85
84
86
86
86
86
86
RCA#1 APPENDIX F
-------
16:33
16:34
16:35
16:36
16:37
16:38
16:39
16:40
16:41
16:42
16:43
16:44
16:45
16:46
16:47
16:48
16:49
16:50
16:51
16:52
16:53
16:54
16:55
16:56
16:57
16:58
16:59
17:00
17:01
17:02
17:03
17:04
17:05
17:06
17:07
17:08
17:09
17:10
17:11
17:12
17:13
17:14
17:15
17:16
17:17
17:18
17:19
17:20
17:21
17:22
17:23
17:24
15.84
16.57
16.99
15.70
15.25
15.96
14.72
13.27
14.09
14.60
15.39
18.40
19.56
13.54
12.97
13.38
13.52
14.15
14.80
15.30
14.40
15.45
15.62
14.88
14.58
15.30
14.56
12.65
14.02
13.48
14.96
17.48
17.76
15.59
12.09
13.25
13.20
14.31
14.94
15.48
14.63
15.32
15.24
15.21
14.58
14.53
15.22
12.47
12.71
13.27
12.92
16.97
26.59
29.44
30.19
27.64
27.79
29.02
31.69
40.84
41.71
41.23
25.33
28.54
30.22
28.54
32.44
33.52
30.37
25.66
24.88
26.05
26.59
26.53
27.37
25.69
25.36
26.65
27.79
36.10
38.41
37.33
25.30
26.59
28.00
24.64
30.34
31.63
30.19
26.29
27.07
26.47
25.60
26.62
26.98
25.93
24.40
25.39
26.53
31.96
36.22
34.81
25.33
23.89
14.56
14.96
14.96
14.96
14.96
14.96
14.96
14.96
14.96
14.96
14.96
14.96
14.96
14.96
15.02
15.04
15.04
15.04
15.04
15.04
15.04
15.04
15.04
15.04
15.04
15.04
15.04
14.40
13.76
13.76
13.76
13.76
13.76
13.76
13.76
13.76
13.76
13.76
13.76
13.76
14.12
15.21
15.21
15.21
15.21
15.21
15.21
15.21
15.21
15.21
15.21
15.21
14.97
15.09
15.14
14.59
14.81
14.69
14.69
14.57
14.81
14.81
14.71
14.65
14.65
14.65
14.77
14.77
14.65
14.77
14.65
14.77
14.53
14.65
14.65
14.40
14.40
14.47
14.48
14.44
14.51
14.53
14.65
14.53
14.53
14.53
14.53
14.53
14.40
14.53
14.39
14.44
14.08
14.44
14.44
14.08
14.20
14.32
14.32
14.20
14.20
14.20
14.20
14.20
85
85
86
85
84
84
84
84
84
84
85
86
86
86
86
86
86
86
86
86
86
86
86
86
86
85
85
84
86
86
86
86
86
86
86
86
86
86
86
84
84
84
84
84
84
84
84
84
84
84
84
84
RCA#1 APPENDIX F
-------
17:25
17:26
17:27
17:28
17:29
17:30
17:31
17:32
17:33
17:34
17:35
17:36
17:37
17:38
17:39
17:40
17:41
17:42
17:43
17:44
17:45
17:46
17:47
17:48
17:49
17:50
17:51
17:52
17.78
16.50
11.49
11.75
12.12
12.99
13.38
14.37
13.35
13.88
14.09
25.21
24.46
25.45
27.22
28.84
21.25
22.81
23.50
22.87
23.38
24.79
15.21
15.21
13.13
13.13
13.13
13.13
13.13
13.13
13.13
13.13
13.13
13.13
13.13
13.13
13.13
12.70
12.56
12.56
12.56
12.56
12.56
12.56
12.56
12.56
12.56
12.56
12.56
12.56
14.20
14.08
14.08
14.08
13.96
14.08
14.20
14.20
14.08
14.20
14.08
84
84
84
84
84
84
84
84
84
84
84
Average
Minimum
Maximum
14.66
11.49
19.56
ESC P5B
28.77
21.25
43.12
DR 300-40
14.20
12.56
15.21
F904K
14.69
13.96
15.17
Moisture
Run 1
84.71
84.00
86.00
Temp
184
For P5B &
M17 300-40
Results mg/acm
Train A
Train B
Average
29.31
26.87
28.09
For F904K
&RSD
mg/dscm
44.9
41.2
43.05
Moisture
%
14.3
14.3
14.3
RCA#1 APPENDIX F
-------
RCA #1 Testing - Run 2: Low PM concentration
8/27/99 ESC P5B Durag 300-40 Durag F904K
Time raw mA raw ra mA raw mA
8:52
8:53
8:54
8:55
8:56
8:57
8:58
8:59
9:00
9:01
9:02
9:03
9:04
9:05
9:06
9:07
9:08
9:09
9:10
9:11
9:12
9:13
9:14
9:15
9:16
9:17
9:18
9:19
9:20
9:21
9:22
9:23
9:24
9:25
9:26
9:27
9:28
9:29
9:30
9:31
9:32
9:33
9:34
9:35
9:36
9:37
9:38
9:39
9:40
6.31
6.37
6.29
6.03
6.16
6.12
6.16
6.26
6.27
6.26
6.22
6.25
6.31
6.23
6.23
6.22
6.40
6.53
6.57
6.78
6.39
6.37
6.38
6.38
6.43
6.48
6.24
6.22
6.31
6.29
6.20
6.32
6.27
6.23
6.34
6.27
6.32
6.53
7.09
6.77
6.55
6.29
7.20
6.30
6.41
6.47
6.34
6.32
6.31
5.65
5.57
5.93
4.95
5.34
4.99
5.29
5.52
5.54
5.73
5.61
5.54
5.69
6.36
6.76
6.66
5.73
5.45
5.43
6.10
6.78
6.77
7.42
5.96
5.96
6.05
6.14
5.62
5.60
5.98
5.57
5.69
5.84
6.43
7.89
6.99
6.25
5.51
5.75
6.00
6.66
6.81
8.03
5.90
6.18
6.13
6.38
5.61
5.73
5.22
5.22
5.22
5.22
5.22
5.22
5.22
5.22
5.22
5.22
5.22
5.22
5.14
5.05
5.05
5.05
5.05
5.05
5.05
5.05
5.05
5.05
5.05
5.05
5.05
5.00
4.82
4.82
4.82
4.82
4.82
4.82
4.82
4.82
4.82
4.82
4.82
4.82
Moisture g/acm H2O Temp.
% Vdc deg C
14.16
14.16
14.04
14.16
14.16
14.16
14.28
14.16
14.12
13.72
13.84
13.84
13.84
13.84
13.84
13.84
13.84
13.96
14.08
14.08
14.08
14.20
13.90
14.12
14.04
14.04
13.91
14.16
14.28
14.16
14.40
14.53
14.53
14.40
14.28
14.24
14.23
14.20
14.20
14.20
14.20
14.32
14.08
14.44
14.32
14.57
14.57
14.69
14.57
86
86
86
86
86
86
86
86
85
84
84
84
84
84
84
84
84
84
84
84
84
84
86
85
86
86
86
86
86
86
86
86
86
86
86
85
85
84
84
84
84
84
84
84
84
84
84
84
84
RCA#1 APPENDIX F
-------
9:41
9:42
9:43
9:44
9:45
9:46
9:47
9:48
9:49
9:50
9:51
9:52
9:53
9:54
9:55
9:56
9:57
9:58
9:59
10:00
10:01
10:02
10:03
10:04
10:05
10:06
10:07
10:08
10:09
10:10
10:11
10:12
10:13
10:14
10:15
10:16
10:17
10:18
10:19
10:20
10:21
10:22
10:23
10:24
10:25
10:26
10:27
10:28
10:29
10:30
10:31
10:32
6.45
6.26
6.30
6.28
6.34
6.27
6.20
6.34
6.47
6.59
7.05
6.45
6.35
6.49
6.34
6.74
6.42
6.38
6.23
6.23
6.25
6.16
6.18
6.16
6.21
6.15
6.13
6.37
6.28
6.47
6.53
6.64
6.35
6.53
6.32
6.45
6.53
6.62
6.23
6.29
6.35
6.27
6.20
6.21
6.55
6.15
6.25
6.24
6.67
6.55
6.64
6.86
6.77
6.01
5.69
5.77
6.14
7.19
7.04
6.76
5.50
5.55
5.89
6.80
7.04
7.19
7.14
6.30
6.00
6.60
5.43
5.41
5.44
5.51
5.40
5.43
5.66
6.00
6.11
6.21
5.17
5.35
5.47
6.45
6.71
7.14
7.07
6.16
6.15
6.15
6.05
5.63
5.64
5.65
5.59
5.66
5.86
6.94
7.42
7.16
6.01
5.54
5.64
6.32
4.90
5.14
5.14
5.14
5.14
5.14
5.14
5.14
5.14
5.14
5.14
5.14
5.14
5.14
4.82
4.82
4.82
4.82
4.82
4.82
4.82
4.82
4.82
4.82
4.82
4.82
4.82
4.82
4.82
4.82
4.82
4.82
4.82
4.82
4.82
4.82
4.82
4.82
4.82
4.82
5.02
5.22
5.22
5.22
5.22
5.22
5.22
5.22
5.22
5.22
5.22
5.22
14.44
13.96
14.32
14.32
14.20
14.20
14.32
14.44
14.32
14.57
14.44
14.39
14.04
13.79
13.62
13.96
13.96
13.84
13.72
13.59
13.47
13.11
13.59
14.08
14.20
14.32
14.69
14.93
14.97
15.01
14.89
14.89
14.77
14.65
14.40
14.65
14.65
14.59
14.32
14.69
14.57
14.44
14.57
14.69
14.81
14.69
14.57
14.44
14.44
14.32
14.32
14.32
84
84
84
84
84
84
84
84
84
84
84
86
86
86
85
84
84
84
84
84
84
84
84
84
84
84
84
84
85
86
86
86
86
86
86
86
86
85
84
84
84
84
84
84
84
84
84
84
84
84
84
84
RCA#1 APPENDIX F
-------
10:33
10:34
10:35
10:36
10:37
10:38
10:39
10:40
10:41
10:42
10:43
10:44
10:45
10:46
10:47
10:48
10:49
10:50
10:51
10:52
10:53
10:54
10:55
10:56
10:57
10:58
10:59
11:00
Average
Minimum
Maximum
Run 2
M17
Results
Train A
Train B
Average
6.38 7.07
6.40 6.95
6.27 7.35
6.36 6.01
6.41 6.08
6.45 6.12
6.32 6.23
6.27 5.75
6.28 5.82
6.82 6.71
6.38 5.71
6.38 6.11
6.03 4.95
7.20 8.03
ESC P5B DR 300-40
For P5B &
300-40
mg/acm
1.92
1.87
1.895
5.22
5.18
5.05
5.05
5.05
5.05
5.05
5.05
5.05
5.05
5.05
5.05
5.05
5.05
5.05
5.22
5.22
5.22
5.22
5.22
5.22
5.22
5.22
5.22
5.22
5.22
5.22
5.22
5.04
4.82
5.22
F904K
For F904K
&RSD
mg/dscm
2.9
2.9
2.9
14.48
14.53
14.40
14.65
14.65
14.65
14.53
14.65
14.53
14.16
14.10
14.28
13.11
15.01
Moisture
Moisture
%
14.09
14.19
14.14
85
86
86
86
86
86
86
86
86
86
85
84.79
84.00
86.00
Temp
185
RCA#1 APPENDIX F
-------
RCA #1 Testing - Run 3: Low PM concentration
8/27/99 ESC P5B Durag 300-40 Durag F904K Moisture g/acm H2O Temp.
Time raw mA raw ra mA raw mA % Vdc deg C
11:44
11:45
11:46
11:47
11:48
11:49
11:50
11:51
11:52
11:53
11:54
11:55
11:56
11:57
11:58
11:59
12:00
12:01
12:02
12:03
12:04
12:05
12:06
12:07
12:08
12:09
12:10
12:11
12:12
12:13
12:14
12:15
12:16
12:17
12:18
12:19
12:20
12:21
12:22
12:23
12:24
12:25
12:26
12:27
12:28
12:29
12:30
12:31
12:32
6.36
6.46
6.49
6.21
6.35
6.33
6.38
6.54
6.65
7.08
6.46
6.38
6.52
6.44
7.30
6.49
6.46
6.36
6.52
6.53
6.52
6.43
6.51
6.50
6.26
6.38
6.41
6.61
6.84
7.05
6.78
6.54
6.65
6.50
6.44
6.56
6.64
6.33
6.38
6.43
6.48
6.41
6.54
6.44
6.24
6.27
6.28
6.48
6.65
6.05
6.12
6.23
7.67
8.07
7.78
7.27
5.78
6.01
6.34
7.53
6.99
7.59
7.64
7.12
6.53
7.17
6.12
6.37
6.42
6.57
6.40
6.62
6.94
8.31
8.35
8.23
6.01
6.26
6.90
7.30
7.78
7.91
7.90
6.69
6.71
6.81
6.70
6.07
6.17
6.61
6.43
6.40
6.39
8.77
7.94
7.80
6.28
5.91
5.22
5.22
5.22
5.22
5.22
5.22
5.22
5.22
5.22
5.22
5.22
5.22
5.22
5.09
5.05
5.05
5.05
5.05
5.05
5.05
5.05
5.05
5.05
5.05
5.05
5.05
5.10
5.14
5.14
5.14
5.14
5.14
5.14
5.14
5.14
5.14
5.14
5.14
5.14
14.77
14.77
14.77
14.65
14.65
14.65
14.65
14.40
14.40
14.40
14.28
14.40
14.40
14.28
14.28
14.28
14.16
14.28
14.40
14.53
14.04
14.40
14.40
14.53
14.40
14.53
14.53
14.53
14.65
14.77
14.65
14.65
14.65
14.44
14.81
14.69
14.69
14.44
14.44
14.44
13.96
14.12
14.04
14.40
14.53
14.53
14.65
14.65
14.77
86
86
86
86
86
86
86
86
86
86
86
86
86
86
86
86
86
86
86
86
86
86
86
86
86
86
86
86
86
86
86
86
86
84
84
84
84
84
84
84
84
85
86
86
86
86
86
86
86
RCA#1 APPENDIX F
-------
12:33
12:34
12:35
12:36
12:37
12:38
12:39
12:40
12:41
12:42
12:43
12:44
12:45
12:46
12:47
12:48
12:49
12:50
12:51
12:52
12:53
12:54
12:55
12:56
12:57
12:58
12:59
13:00
13:01
13:02
13:03
13:04
13:05
13:08
13:09
13:10
13:11
13:12
13:13
13:14
13:15
13:15
13:16
13:16
13:17
13:18
13:20
13:20
13:21
13:22
13:25
13:26
6.73
6.66
6.33
6.26
6.35
6.34
6.50
6.52
6.25
6.27
7.13
6.35
6.19
6.20
6.24
6.16
6.20
6.17
6.24
6.47
6.61
6.58
6.16
6.24
6.45
6.34
6.42
6.37
6.30
6.19
6.23
6.26
6.21
6.22
6.11
6.22
6.17
6.38
6.42
6.56
6.28
6.27
6.29
6.28
6.34
6.13
6.27
6.28
6.32
6.30
6.22
6.18
6.00
6.37
7.24
7.21
7.79
6.18
6.39
6.48
6.37
5.88
6.41
6.28
5.69
5.95
5.90
6.80
7.49
7.16
6.36
5.52
5.56
5.95
6.48
6.72
7.71
6.43
6.24
6.13
6.26
5.61
5.74
5.72
5.66
5.66
6.74
6.82
6.88
5.33
5.44
5.84
6.69
6.66
6.89
6.95
7.17
6.16
5.91
5.93
6.21
6.12
5.88
5.65
5.12
5.05
5.05
5.05
5.05
5.05
5.05
5.05
5.06
5.05
5.05
5.05
5.05
5.05
5.05
5.05
5.05
5.05
5.05
5.05
5.05
5.05
5.05
5.05
5.05
5.06
5.05
5.24
5.30
5.30
5.30
5.30
5.30
5.30
5.30
5.30
5.30
5.30
4.98
4.66
4.66
4.66
4.66
4.66
4.66
4.66
4.66
4.66
4.66
4.66
4.66
4.90
14.77
14.63
14.44
14.44
14.32
14.44
14.44
14.32
14.24
14.28
14.28
14.04
14.16
14.16
14.28
14.28
14.16
14.28
14.28
13.91
13.55
13.30
13.30
13.50
13.38
13.50
13.50
13.62
13.50
13.65
13.82
13.82
13.33
13.33
13.82
13.82
13.95
13.95
13.95
13.82
13.95
13.95
13.95
13.95
13.95
14.03
14.24
14.24
14.24
14.24
13.99
14.24
86
86
84
84
84
84
84
84
85
86
86
86
86
86
86
86
86
86
86
86
86
86
86
88
88
88
88
88
88
89
90
90
90
90
90
90
90
90
90
90
90
90
90
90
90
89
88
88
88
88
88
88
RCA#1 APPENDIX F
-------
13:27
13:28
13:29
13:30
13:31
13:32
13:33
13:34
13:35
13:36
13:37
13:38
13:39
13:40
13:41
13:42
13:43
13:44
13:45
13:46
13:47
13:48
13:49
13:50
13:51
Average
Minimum
Maximum
Run 3
M17
Results
Train A
Train B
Average
6.14 5.67 5.14
6.57 6.83 5.14
6.13 7.00 5.14
6.09 6.91 5.14
6.19 6.91 5.14
6.34 5.47 5.14
6.48 5.55 5.14
6.55 5.62 5.14
5.14
5.14
5.14
5.14
5.12
5.05
5.05
5.05
5.06
5.05
5.05
5.06
5.05
5.05
5.05
5.05
5.05
6.41 6.59 5.07
6.09 5.33 4.66
7.30 8.77 5.30
ESC P5B DR 300-40 F904K
For P5B & For F904K
300-40 & RSD
mg/acm mg/dscm
2.47 3.8
2.62 4.1
2.545 3.95
14.12
14.24
14.24
14.36
14.36
14.48
14.36
14.48
14.24
13.30
14.81
Moisture
Moisture
%
14.26
14.81
14.535
88
88
88
88
88
88
88
88
86.70
84.00
90.00
Temp
188
RCA#1 APPENDIX F
-------
RCA #1 Testing - Run 4: Low PM concentration
8/27/99 ESC P5B Durag 300-40 Durag F904K Moisture g/acm H2O Temp.
Time raw mA raw ra mA raw mA % Vdc deg C
14:48
14:49
14:50
14:51
14:52
14:53
14:54
14:55
14:56
14:57
14:58
14:59
15:00
15:01
15:02
15:03
15:04
15:05
15:06
15:07
15:08
15:09
15:10
15:11
15:12
15:13
15:14
15:15
15:16
15:17
15:18
15:19
15:20
15:21
15:22
15:23
15:24
15:25
15:26
15:27
15:28
15:29
15:30
15:31
15:32
15:33
15:34
15:35
15:36
6.16
6.19
6.26
6.11
6.11
6.22
6.10
6.16
6.18
6.39
6.21
6.57
6.56
6.75
6.28
6.25
6.17
6.28
6.46
6.53
6.12
6.20
6.24
6.23
6.12
6.22
6.44
6.18
6.17
6.29
6.60
6.52
6.66
7.02
6.43
6.52
6.22
6.34
6.36
6.51
6.34
6.35
7.20
6.39
6.19
6.22
6.31
6.17
6.20
5.70
5.72
6.07
5.70
5.75
5.88
6.95
7.34
7.15
6.98
5.33
5.75
5.81
6.54
6.89
6.97
7.36
6.32
6.49
6.35
5.92
5.82
6.04
5.94
5.89
5.99
6.26
8.26
7.71
7.29
6.11
5.87
5.91
6.67
7.62
7.66
8.03
6.47
6.65
6.62
6.48
6.09
7.02
6.29
6.12
6.18
6.21
7.35
8.11
4.82
4.82
4.82
4.82
4.82
4.82
4.82
4.82
4.82
4.82
4.82
4.82
4.82
4.52
4.42
4.42
4.42
4.42
4.42
4.42
4.42
4.42
4.42
4.42
4.42
4.42
4.74
5.05
5.05
5.05
5.05
5.05
5.05
5.05
5.05
5.05
5.05
5.05
14.53
14.53
14.40
14.28
14.53
15.62
16.97
16.97
16.97
18.19
18.19
17.70
16.23
16.11
14.77
14.61
14.32
14.44
14.57
14.57
14.44
14.57
14.57
14.44
14.69
14.77
14.77
14.65
14.53
14.65
14.77
14.65
14.65
14.65
14.53
14.53
14.40
14.65
14.65
14.77
14.65
14.77
14.77
14.59
14.69
14.69
14.69
14.69
14.69
86
86
86
86
86
86
86
86
86
86
86
86
86
86
86
85
84
84
84
84
84
84
84
84
84
86
86
86
86
86
86
86
86
86
86
86
86
86
86
86
86
86
86
85
84
84
84
84
84
10
RCA#1 APPENDIX F
-------
15:37
15:38
15:39
15:40
15:41
15:42
15:43
15:44
15:45
15:46
15:47
15:48
15:49
15:50
15:51
15:52
15:53
15:54
15:55
15:56
15:57
15:58
15:59
16:00
16:01
16:02
16:03
16:04
16:05
16:06
16:07
16:08
16:09
16:10
16:11
16:12
16:13
16:14
16:15
16:16
16:17
16:18
16:19
16:20
16:21
16:22
16:23
16:24
16:25
16:26
16:27
16:28
6.45
6.34
6.63
6.78
6.81
6.30
6.38
7.70
6.62
6.44
6.57
6.42
6.35
6.42
6.42
6.41
6.33
6.35
6.39
6.48
6.27
6.26
6.54
6.85
6.88
6.48
6.38
6.32
7.32
6.45
6.39
6.50
6.22
6.27
6.34
6.30
6.18
6.21
6.44
6.12
6.24
6.17
6.36
6.57
6.65
6.53
6.30
6.21
7.08
6.36
6.45
6.52
8.08
7.12
6.15
6.06
7.15
7.22
7.46
8.38
7.08
6.65
6.67
7.22
6.19
6.26
6.35
6.78
6.48
6.58
7.64
8.40
8.43
8.07
6.08
6.41
6.29
8.51
7.72
7.74
6.99
6.82
6.46
7.30
5.82
6.10
6.16
6.43
6.11
6.16
7.64
7.78
7.77
7.72
5.96
5.89
6.02
7.47
7.37
7.30
7.29
6.54
6.46
6.61
5.05
5.01
4.90
4.90
4.90
4.90
4.90
4.90
4.90
4.90
4.90
4.90
4.90
4.90
4.90
4.66
4.66
4.66
4.66
4.66
4.66
4.66
4.66
4.66
4.66
4.66
4.66
4.66
5.46
5.46
5.46
5.46
5.46
5.45
5.45
5.45
5.45
5.45
5.45
5.45
5.45
5.10
4.98
4.98
4.98
4.98
4.98
4.98
4.98
4.98
4.98
4.98
14.57
14.57
14.57
14.61
14.65
14.65
14.65
14.65
14.65
14.77
14.77
14.65
14.89
14.65
14.65
14.16
14.51
14.61
14.65
14.53
14.53
14.53
14.53
14.53
14.53
14.40
14.40
14.53
14.53
14.53
14.53
14.40
14.53
14.28
14.40
14.04
14.24
14.32
14.20
14.32
14.44
14.44
14.32
14.32
14.32
14.20
14.10
14.16
14.16
14.16
14.28
14.16
84
84
84
85
86
86
86
86
86
86
86
86
86
86
86
86
86
85
86
86
86
86
86
86
86
86
86
86
86
86
86
86
86
86
86
86
85
84
84
84
84
84
84
84
84
84
85
86
86
86
86
86
11
RCA#1 APPENDIX F
-------
16:29
16:30
16:31
16:32
16:33
16:34
16:35
16:36
16:37
16:38
16:39
16:40
16:41
16:42
16:43
16:44
16:45
16:46
16:47
16:48
16:49
16:50
16:51
16:52
16:53
16:54
16:55
16:56
16:57
Average
Minimum
Maximum
Run 4
M17
Results
Train A
Train B
Average
6.29 6.59
6.53 6.87
6.38 6.16
6.29 6.34
6.22 6.09
6.25 6.13
6.27 6.23
6.23 7.81
6.13 7.91
6.21 7.91
6.40 6.75
6.10 5.33
7.70 8.51
ESC P5B DR 300-40
For P5B &
300-40
mg/acm
2.57
2.6
2.585
4.98
4.98
5.34
5.70
5.70
5.70
5.70
5.70
5.70
5.70
5.70
5.70
5.70
5.70
5.70
5.50
4.90
4.90
4.90
4.90
4.90
4.90
4.90
4.90
4.90
4.90
4.90
4.90
4.90
4.99
4.42
5.70
F904K
For F904K
&RSD
mg/dscm
4
4
4
14.28
14.40
14.40
14.04
14.04
14.16
14.27
14.23
14.20
14.20
14.69
14.04
18.19
Moisture
Moisture
%
14.33
14.75
14.54
86
86
86
86
86
86
86
85
84
84
85.43
84.00
86.00
Temp
186
12
RCA#1 APPENDIX F
-------
RCA #1 Testing - Run 5: Medium PM concentration
8/28/99 ESC P5B Durag 300-40 Durag F904K Moisture
Time raw mA raw ra mA raw mA %
8:50
8:51
8:52
8:53
8:54
8:55
8:56
8:57
8:58
8:59
9:00
9:01
9:02
9:03
9:04
9:05
9:06
9:07
9:08
9:09
9:10
9:11
9:12
9:13
9:14
9:15
9:16
9:17
9:18
9:19
9:20
9:21
9:22
9:23
9:24
9:25
9:26
9:27
9:28
9:29
9:30
9:31
9:32
9:33
9:34
9:35
9:36
9:37
9:38
8.69
8.55
7.85
8.27
8.65
8.93
9.79
10.35
9.39
8.65
8.41
11.06
8.58
8.65
8.62
8.38
8.39
8.60
8.81
8.45
8.53
8.72
8.03
7.87
8.54
8.42
9.60
9.99
9.70
8.10
8.05
9.83
8.24
8.61
8.96
8.88
8.74
8.72
8.71
8.57
8.40
8.69
8.14
7.83
7.97
8.05
8.67
9.13
9.59
10.67
10.74
15.01
15.52
15.27
11.71
10.98
11.68
12.70
14.47
14.59
15.52
11.15
10.88
11.17
11.61
10.62
10.76
11.95
10.41
10.93
11.13
14.42
15.41
14.94
12.45
11.05
11.19
13.25
12.58
13.16
14.86
10.62
11.23
11.55
12.30
10.78
11.04
10.98
11.05
10.70
10.99
12.52
14.63
14.39
13.44
8.95
9.96
9.53
7.93
7.93
7.93
7.93
7.93
7.93
7.93
7.93
7.93
7.93
7.93
7.93
7.93
7.30
7.30
7.30
7.30
7.30
7.30
7.30
7.30
7.30
7.30
7.30
7.30
7.30
7.60
7.70
7.70
7.70
7.70
7.70
7.70
7.70
7.70
7.70
7.70
7.70
7.70
16.48
16.84
16.48
17.45
17.45
16.84
15.26
15.26
14.40
14.40
14.28
14.04
13.79
13.47
13.35
13.35
13.72
13.96
14.02
14.14
14.08
13.96
13.72
13.72
13.96
14.04
14.04
13.91
14.04
14.16
14.04
14.04
13.91
14.16
14.04
13.91
14.16
13.91
13.91
13.67
13.78
13.74
13.23
12.87
12.87
13.11
13.23
13.47
13.47
Temp.
degC
86
86
86
86
86
86
86
86
86
86
86
86
86
84
84
84
84
84
86
86
84
84
84
84
84
86
86
86
86
86
86
86
86
86
86
86
86
86
86
86
86
85
84
84
84
84
84
84
84
13
RCA#1 APPENDIX F
-------
9:39
9:40
9:41
9:42
9:43
9:44
9:45
9:46
9:47
9:48
9:49
9:50
9:51
9:52
9:53
9:54
9:55
9:56
9:57
9:58
9:59
10:00
10:01
10:02
10:03
10:04
10:05
10:06
10:07
10:08
10:09
10:10
10:11
10:12
10:13
10:14
10:15
10:16
10:17
10:18
10:19
10:20
10:21
10:22
10:23
10:24
10:25
10:26
10:27
10:28
10:29
10:30
7.39
7.67
7.61
8.45
7.89
8.04
8.20
7.50
8.24
8.23
8.28
8.36
8.27
8.39
8.05
7.98
7.96
8.49
9.28
9.75
10.02
7.87
8.04
8.28
7.78
8.27
8.36
8.89
8.12
8.36
8.54
8.35
8.27
8.42
8.13
7.57
7.98
8.12
8.51
9.46
9.41
8.37
7.68
7.90
7.54
8.28
8.33
8.89
8.57
8.43
8.53
8.42
10.57
11.02
11.81
9.99
9.11
9.74
10.68
8.30
9.45
10.14
10.32
10.00
10.04
10.46
11.86
15.37
15.18
15.30
10.34
10.96
11.16
13.69
13.20
13.30
10.64
10.98
10.73
11.81
9.51
10.23
10.61
9.98
10.31
10.35
11.48
13.58
13.90
14.35
9.84
9.93
10.52
12.35
12.38
12.51
11.30
10.63
10.96
11.14
10.79
10.25
10.46
10.54
7.21
7.05
7.05
7.05
7.05
7.05
7.05
7.05
7.05
7.05
7.05
7.05
7.05
6.62
6.18
6.18
6.18
6.18
6.18
6.18
6.18
6.18
6.18
6.18
6.18
6.18
6.50
7.45
7.45
7.45
7.45
7.45
7.45
7.45
7.45
7.45
7.45
7.45
7.45
7.45
7.45
7.45
7.45
7.45
7.45
7.45
7.45
7.45
7.45
7.45
7.45
7.45
13.59
13.72
14.04
13.91
14.04
14.04
14.04
13.91
14.04
14.28
14.28
13.91
14.08
14.08
14.08
13.84
13.96
13.96
13.84
13.84
13.96
13.84
13.72
13.51
13.30
13.51
13.78
13.79
13.91
14.04
13.91
13.55
13.66
13.72
13.72
13.59
13.72
13.59
13.47
13.59
13.59
13.72
13.72
13.79
13.67
13.91
14.04
14.04
13.79
13.67
13.43
13.43
84
84
86
86
86
86
86
86
86
86
86
86
84
84
84
84
84
84
84
84
84
84
84
85
86
85
86
86
86
86
86
86
86
84
84
84
84
84
84
84
84
84
84
86
86
86
86
86
86
86
86
86
14
RCA#1 APPENDIX F
-------
10:31
10:32
10:33
10:34
10:35
10:36
10:37
10:38
10:39
10:40
10:41
10:42
10:43
10:44
10:45
10:46
10:47
10:48
10:49
10:50
10:51
10:52
10:53
10:54
10:55
10:56
10:57
Average
Minimum
Maximum
Run 5
M17
Results
Train A
Train B
Average
8.26 9.91
8.35 10.36
8.25 10.62
7.60 14.33
7.73 14.91
8.20 14.76
8.40 11.14
9.57 9.96
9.79 10.77
8.77 12.50
8.51 11.72
7.39 8.30
11.06 15.52
ESC P5B DR 300-40
For P5B &
300-40
mg/acm
9.62
9.92
9.77
7.45
7.70
7.78
7.78
7.78
7.78
7.78
7.78
7.78
7.78
7.78
7.78
7.78
7.78
7.34
6.90
6.90
6.90
6.90
6.90
6.90
6.90
6.90
6.90
6.90
6.90
6.90
7.30
6.18
7.93
F904K
For F904K
&RSD
mg/dscm
14.6
15
14.8
13.55
13.67
13.67
13.67
13.66
13.59
13.72
13.72
13.96
13.96
14.00
12.87
17.45
Moisture
Moisture
%
14.1
13.7
13.9
86
86
86
86
86
84
84
84
84
84
85.16
84.00
86.00
Temp
185
RCA#1 APPENDIX F
15
-------
RCA #1 Testing - Run 6: Medium PM concentration
8/28/99 ESC P5B Durag 300-40 Durag F904K Moisture
Time raw mA raw ra mA raw mA %
11:41
11:42
11:43
11:44
11:45
11:46
11:47
11:48
11:49
11:50
11:51
11:52
11:53
11:54
11:55
11:56
11:57
11:58
11:59
12:00
12:01
12:02
12:03
12:04
12:05
12:06
12:07
12:08
12:09
12:10
12:11
12:12
12:13
12:14
12:15
12:16
12:17
12:18
12:19
12:20
12:21
12:22
12:23
12:24
12:25
12:26
12:27
12:28
12:29
7.01
7.29
7.36
7.17
7.52
7.77
8.09
7.34
7.47
7.67
7.86
8.54
8.55
8.68
8.25
8.37
8.78
7.92
7.82
8.29
8.34
9.49
9.82
9.30
7.70
8.03
8.84
7.64
8.06
8.20
8.03
8.41
8.44
8.52
8.36
8.30
8.20
7.91
7.48
7.86
8.26
8.87
9.13
9.52
7.62
7.47
7.71
8.45
7.94
9.51
10.33
10.51
9.10
9.01
9.29
9.86
7.96
8.35
8.69
9.19
10.95
11.30
12.07
10.89
11.56
11.84
13.90
17.48
16.39
12.86
10.87
11.53
11.81
11.98
13.02
14.35
10.47
10.85
10.88
10.90
10.27
10.69
11.10
10.80
10.59
11.25
12.46
15.85
15.46
13.54
10.07
10.71
11.17
11.34
12.38
12.18
11.00
10.48
6.72
6.42
6.42
6.42
6.42
6.42
6.42
6.42
6.42
6.42
6.42
6.42
6.42
7.02
7.62
7.62
7.62
7.62
7.62
7.62
7.62
7.62
7.62
7.62
7.62
7.62
7.34
6.50
6.50
6.50
6.50
6.50
6.50
6.50
6.50
6.50
6.50
6.50
6.50
13.47
13.78
13.91
14.04
14.28
14.40
14.40
14.28
14.28
14.40
14.40
14.53
14.65
14.28
14.28
14.16
14.16
14.04
14.04
14.04
13.91
13.79
13.67
13.59
13.63
13.67
13.55
13.79
13.79
13.79
13.79
14.04
14.04
14.16
13.79
14.16
14.04
14.04
13.79
13.79
13.91
14.04
13.91
14.04
13.91
13.79
13.91
13.91
14.16
Temp.
degC
84
86
86
86
86
86
86
86
86
86
86
86
86
86
86
86
86
86
86
86
86
86
86
84
85
86
86
86
86
86
86
86
86
86
86
86
86
86
86
86
86
86
86
86
86
86
86
86
86
RCA#1 APPENDIX F
-------
12:30
12:31
12:32
12:33
12:34
12:35
12:36
12:37
12:38
12:39
12:40
12:41
12:42
12:43
12:44
12:45
12:46
12:47
12:48
12:49
12:50
12:51
12:52
12:53
12:54
12:55
12:56
12:57
12:58
12:59
13:00
13:01
13:02
13:03
13:04
13:05
13:06
13:07
13:08
13:09
13:10
13:11
13:12
13:13
13:14
13:15
13:16
13:17
13:18
13:19
13:20
13:21
8.28
8.15
8.09
8.29
8.42
7.97
7.97
8.09
8.16
7.41
7.60
7.87
8.47
9.21
9.65
8.19
7.71
7.78
9.16
8.09
8.26
8.53
8.07
8.33
8.30
8.32
8.17
8.18
8.49
7.86
8.12
8.18
8.51
9.59
10.14
9.23
8.11
8.06
9.37
8.31
8.48
8.92
8.67
8.84
8.91
9.05
8.63
8.84
9.03
8.36
8.24
8.55
10.73
11.90
9.62
10.30
10.62
10.42
10.29
10.41
11.46
14.66
15.05
15.08
9.64
10.65
10.88
12.10
12.53
13.37
12.42
11.22
11.21
11.05
10.66
10.42
10.64
10.71
10.31
10.79
11.26
14.60
15.92
16.09
11.85
10.85
11.28
12.75
13.87
14.21
14.30
11.81
11.83
11.95
11.99
11.79
12.14
12.75
11.36
11.53
12.10
15.23
18.00
18.06
6.50
7.22
7.22
7.22
7.22
7.22
7.22
7.22
7.22
7.22
7.22
7.22
7.22
7.22
7.22
7.22
7.22
7.22
7.22
7.22
7.22
7.22
7.22
7.22
7.22
7.22
7.22
6.74
6.25
6.25
6.25
6.25
6.25
6.25
6.25
6.25
6.25
6.25
6.25
6.25
6.55
7.45
7.45
7.45
7.45
7.45
7.45
7.45
7.45
7.45
7.45
7.45
14.28
14.16
14.28
14.40
14.28
13.79
14.04
14.04
14.04
13.91
14.04
14.04
14.04
13.91
14.04
13.91
14.04
13.91
13.79
13.79
13.79
13.67
13.43
13.61
13.75
13.26
13.38
13.50
13.62
13.50
13.62
13.75
13.62
13.62
13.62
13.62
13.54
13.58
13.58
13.45
13.45
13.21
13.45
13.58
13.58
13.33
13.58
13.45
13.58
13.58
13.70
13.70
86
86
86
86
86
86
86
86
86
86
86
86
86
86
86
86
86
86
86
86
86
86
86
88
88
88
88
88
88
88
88
88
88
88
88
88
89
90
90
90
90
90
90
90
90
90
90
90
90
90
90
90
17
RCA#1 APPENDIX F
-------
13:22
13:23
13:24
13:25
13:26
13:27
13:28
13:29
13:30
13:31
13:32
13:33
13:34
13:35
13:36
13:37
13:38
13:39
13:40
13:41
13:42
13:43
13:44
13:45
13:46
13:47
13:48
13:49
Average
Minimum
Maximum
Run 6
M17
Results
Train A
Train B
Average
8.29 14.45
9.61 11.68
9.81 11.91
9.61 13.15
8.03 12.95
8.05 13.44
9.41 15.35
7.89 11.35
8.30 11.24
8.46 11.59
8.35 11.92
7.01 7.96
10.14 18.06
ESC P5B DR 300-40
For P5B &
300-40
mg/acm
8.25
8.33
8.29
7.45
7.45
7.05
7.05
7.05
7.05
7.05
7.05
7.05
7.05
7.05
7.05
7.05
7.05
7.05
7.18
7.22
7.22
7.22
7.22
7.22
7.22
7.22
7.22
7.22
7.22
7.22
7.22
6.99
6.25
7.62
F904K
For F904K
&RSD
mg/dscm
12.6
12.7
12.65
13.82
13.68
13.62
13.75
13.62
13.62
13.62
13.62
13.62
13.62
13.85
13.21
14.65
Moisture
Moisture
%
13.8
13.9
13.85
90
90
88
88
88
88
88
88
88
88
86.97
84.00
90.00
Temp
189
18
RCA#1 APPENDIX F
-------
RCA #1 Testing - Run 7: Mid PM concentration
8/28/99 ESC P5B Durag 300-40 Durag F904K Moisture
Time raw mA raw ra mA raw mA %
15:00
15:01
15:02
15:03
15:04
15:05
15:06
15:07
15:08
15:09
15:10
15:11
15:12
15:13
15:14
15:15
15:16
15:17
15:18
15:19
15:20
15:21
15:22
15:23
15:24
15:25
15:26
15:27
15:28
15:29
15:30
15:31
15:32
15:33
15:34
15:35
15:36
15:37
15:38
15:39
15:40
15:41
15:42
15:43
15:44
15:45
15:46
15:47
15:48
7.29
7.47
7.39
7.63
8.25
8.76
9.07
7.26
7.21
7.31
7.11
7.52
7.65
8.01
7.40
7.52
7.49
7.59
7.35
7.45
7.36
7.00
7.38
7.45
7.97
8.67
8.94
7.75
7.32
7.60
7.12
7.55
7.70
7.92
7.91
7.61
7.63
7.75
7.49
7.56
7.80
6.96
7.25
7.36
7.84
8.48
8.94
8.24
7.62
11.42
13.97
14.05
12.92
9.20
9.70
10.11
10.67
10.65
10.72
9.57
9.52
9.52
10.26
8.48
8.80
9.09
8.81
9.28
9.36
10.15
12.64
13.17
13.07
9.03
9.48
9.70
10.86
10.92
11.36
10.39
9.64
9.63
10.07
9.23
9.25
9.35
9.58
9.26
9.81
10.20
13.32
14.11
13.68
10.91
9.62
10.15
11.93
11.72
6.90
6.90
6.90
6.90
6.90
6.90
6.90
6.90
6.90
6.90
6.90
6.90
6.90
6.73
6.73
6.73
6.73
6.73
6.73
6.73
6.73
6.73
6.73
6.73
6.73
6.73
6.67
6.65
6.65
6.65
6.65
6.65
6.65
6.65
6.65
6.65
6.65
6.65
6.65
13.86
13.82
13.82
13.95
13.82
13.82
13.78
13.75
13.75
13.87
13.87
13.87
13.87
13.87
14.12
13.99
13.75
13.75
13.87
13.99
13.85
13.91
13.79
14.04
14.04
14.04
14.16
14.16
14.04
14.16
14.16
14.16
14.16
14.16
14.16
14.28
14.28
14.16
14.16
14.16
14.28
14.16
13.79
13.91
13.79
13.91
14.04
14.16
14.16
Temp.
degC
91
90
90
90
90
90
89
88
88
88
88
88
88
88
88
88
88
88
88
88
88
86
86
86
86
86
86
86
86
86
86
86
86
86
86
86
86
86
86
86
86
86
86
86
86
86
86
86
86
19
RCA#1 APPENDIX F
-------
15:49
15:50
15:51
15:52
15:53
15:54
15:55
15:56
15:57
15:58
15:59
16:00
16:01
16:02
16:03
16:04
16:05
16:06
16:07
16:08
16:09
16:10
16:11
16:12
16:13
16:14
16:15
16:16
16:17
16:18
16:19
16:20
16:21
16:22
16:23
16:24
16:25
16:26
16:27
16:28
16:29
16:30
16:31
16:32
16:33
16:34
16:35
16:36
16:37
16:38
16:39
16:40
7.48
7.55
7.52
7.84
8.06
8.26
7.91
7.98
8.43
7.92
7.98
8.03
7.47
7.23
7.40
7.35
8.58
8.90
8.59
7.24
7.31
7.62
7.17
7.48
7.73
8.32
7.80
7.99
8.25
8.33
7.76
7.85
7.07
6.84
7.09
7.37
7.91
8.72
8.95
7.38
7.59
7.71
7.24
7.50
7.84
8.88
7.30
7.86
8.38
8.67
8.07
7.94
11.77
12.17
10.36
10.65
10.48
10.40
10.00
10.24
11.09
9.93
10.67
10.83
12.97
15.01
14.15
12.50
9.82
10.23
11.82
10.91
11.65
11.90
9.62
10.04
10.41
10.55
9.60
10.34
11.07
10.72
9.90
10.38
10.77
11.56
12.07
12.02
8.65
9.74
10.31
12.65
12.05
12.83
10.25
9.12
9.76
10.50
8.88
9.80
10.96
10.45
10.55
10.42
7.09
7.53
7.53
7.53
7.53
7.53
7.53
7.53
7.53
7.53
7.53
7.53
7.53
7.38
7.22
7.22
7.22
7.22
7.22
7.22
7.22
7.22
7.22
7.22
7.22
7.22
7.08
6.65
6.65
6.65
6.65
6.65
6.65
6.65
6.65
6.65
6.65
6.65
6.65
6.65
6.25
6.25
6.25
6.25
6.25
6.25
6.25
6.25
6.25
6.25
6.25
6.25
14.16
14.16
14.16
14.04
14.16
14.04
14.16
14.16
14.04
13.79
13.79
13.79
13.67
12.94
13.55
13.79
13.91
14.16
14.40
14.40
14.28
14.16
14.04
14.16
14.16
14.16
14.28
14.40
14.40
14.16
14.04
13.79
11.96
11.00
11.08
11.19
11.40
11.59
11.40
11.32
11.22
11.14
10.78
10.31
10.61
10.90
10.55
10.94
12.11
12.11
12.31
12.40
86
86
86
86
86
86
86
86
86
86
86
86
86
86
86
86
86
86
86
86
86
86
86
86
86
86
86
86
86
86
86
86
86
87
89
93
96
98
100
101
102
104
105
106
108
109
110
110
110
110
108
107
20
RCA#1 APPENDIX F
-------
16:41
16:42
16:43
16:44
16:45
16:46
16:47
16:48
16:49
16:50
16:51
16:52
16:53
16:54
16:55
16:56
16:57
16:58
16:59
17:00
17:01
17:02
17:03
17:04
17:05
17:06
17:07
Average
Minimum
Maximum
7.97
7.08
7.50
7.62
7.94
8.69
8.93
7.72
7.47
7.47
7.77
6.84
9.07
ESC P5B
10.77
12.96
13.44
14.05
9.86
9.87
10.30
10.80
11.43
11.61
10.80
8.48
15.01
DR 300-40
6.25
6.38
6.42
6.42
6.42
6.42
6.42
6.42
6.42
6.42
6.42
6.42
6.42
6.42
7.02
7.62
7.62
7.62
7.62
7.62
7.62
7.62
7.62
7.62
7.62
7.62
7.62
6.88
6.25
7.62
F904K
12.50
12.31
12.69
12.77
12.50
13.13
13.70
13.79
14.00
14.05
13.45
10.31
14.40
Moisture
106
104
104
103
102
102
100
99
98
96
90.77
86.00
110.00
Temp
195
Run 7
For P5B &
M17 300-40
Results mg/acm
Train A
Train B
Average
11.45
11.14
11.295
For F904K
&RSD
mg/dscm
17.6
17.2
17.4
Moisture
%
13.7
14
13.85
RCA#1 APPENDIX F
21
-------
RCA #1 Testing - Run 8: Mid-high PM concentration
8/29/99 ESC P5B Durag 300-40 Durag F904K Moisture
Time raw mA raw ra mA raw mA %
9:14
9:15
9:16
9:17
9:18
9:19
9:20
9:21
9:22
9:23
9:24
9:25
9:26
9:27
9:28
9:29
9:30
9:31
9:32
9:33
9:34
9:35
9:36
9:37
9:38
9:39
9:40
9:41
9:42
9:43
9:44
9:45
9:46
9:47
9:48
9:49
9:50
9:51
9:52
9:53
9:54
9:55
9:56
9:57
9:58
9:59
10:00
10:01
10:02
9.14
8.83
9.46
9.58
10.24
8.80
8.67
8.92
9.34
9.55
10.24
10.63
10.11
10.48
10.19
10.19
9.40
10.29
10.35
10.47
12.91
12.69
10.36
9.18
9.25
8.98
9.85
10.20
10.32
9.81
10.03
10.10
10.30
10.19
10.04
10.33
10.01
9.20
9.46
9.82
12.09
12.34
11.19
8.95
9.21
9.26
9.72
10.17
10.15
16.55
13.56
13.07
13.14
13.44
10.51
10.57
10.93
10.95
12.79
14.37
14.98
13.78
14.75
15.42
16.00
19.51
21.46
21.49
15.19
15.23
15.80
15.91
17.42
17.87
17.25
14.65
14.97
14.73
13.29
14.31
15.06
14.78
13.67
14.99
15.28
17.38
20.89
20.65
16.51
14.31
14.87
14.88
15.67
16.93
17.16
13.74
14.36
13.98
9.30
9.30
9.30
9.30
9.30
9.30
9.30
9.30
9.30
9.30
9.30
9.30
9.46
9.61
9.61
9.61
9.61
9.61
9.61
9.61
9.61
9.61
9.61
9.61
9.61
9.53
9.30
9.30
9.30
9.30
9.30
9.30
9.30
9.30
9.30
9.30
9.30
9.30
9.30
14.04
13.91
14.04
14.04
13.91
13.79
13.91
14.16
14.28
14.40
14.40
14.40
14.04
14.16
14.16
14.28
14.28
14.28
14.28
14.40
14.40
14.40
14.36
14.20
14.32
14.08
14.20
14.20
14.20
14.08
14.20
14.28
14.04
14.04
14.04
14.04
14.16
14.16
14.04
14.16
14.28
14.28
14.28
14.40
14.40
14.28
14.40
14.47
14.32
Temp.
deg C
86
86
86
86
86
86
86
86
86
86
86
86
86
86
86
86
86
86
86
86
86
86
85
84
84
84
84
84
84
84
84
86
86
86
86
86
86
86
86
86
86
86
86
86
86
86
86
85
84
22
RCA#1 APPENDIX F
-------
10:03
10:04
10:05
10:06
10:07
10:08
10:09
10:10
10:11
10:12
10:13
10:14
10:15
10:16
10:17
10:18
10:19
10:20
10:21
10:22
10:23
10:24
10:25
10:26
10:27
10:28
10:29
10:30
10:31
10:32
10:33
10:34
10:35
10:36
10:37
10:38
10:39
10:40
10:41
10:42
10:43
10:44
10:45
10:46
10:47
10:48
10:49
10:50
10:51
10:52
10:53
10:54
9.96
10.13
9.94
10.36
10.19
10.27
10.54
9.77
9.58
9.74
9.83
12.11
13.19
13.40
9.38
9.55
9.25
10.20
10.14
10.42
10.80
10.53
11.06
11.37
10.58
10.74
11.13
10.53
9.61
10.34
10.57
11.71
13.20
13.53
10.38
9.73
10.12
10.21
10.58
10.60
11.33
10.43
10.79
11.04
10.83
10.67
10.57
10.75
9.13
9.44
9.77
10.83
13.07
13.51
14.30
15.02
13.78
15.08
15.91
16.75
22.57
22.99
20.92
15.64
16.34
16.94
15.46
17.85
18.46
16.03
15.19
16.01
16.43
14.85
16.66
17.54
16.13
16.41
16.66
18.13
23.44
24.22
24.25
14.54
17.01
17.14
16.44
18.57
18.55
18.04
16.19
15.88
16.07
15.35
15.76
16.06
15.44
15.19
15.63
16.36
20.50
22.39
21.28
14.78
9.69
9.69
9.69
9.69
9.69
9.69
9.69
9.69
9.69
9.69
9.69
9.69
9.69
9.10
8.90
8.90
8.90
8.90
8.90
8.90
8.90
8.90
8.90
8.90
8.90
8.90
9.38
9.85
9.85
9.85
9.85
9.85
9.85
9.85
9.85
9.85
9.85
9.85
9.85
10.11
10.89
10.89
10.89
10.89
10.89
10.89
10.89
10.89
10.89
10.89
10.89
10.89
14.32
14.44
14.32
14.35
14.04
14.40
14.40
14.40
14.40
14.40
14.53
14.53
14.28
13.91
13.91
14.04
14.16
14.16
14.40
14.53
14.28
14.53
14.53
14.53
14.16
14.16
14.28
14.40
14.28
14.40
14.53
14.53
14.53
14.53
14.40
14.40
14.28
14.16
14.10
14.08
14.08
13.90
14.16
14.04
13.67
13.91
14.04
14.16
14.04
14.16
14.16
14.16
84
84
84
85
86
86
86
86
86
86
86
86
86
86
86
86
86
86
86
86
86
86
86
86
86
86
86
86
86
86
86
86
86
86
86
86
86
86
85
84
84
86
86
86
86
86
86
86
86
86
86
86
23
RCA#1 APPENDIX F
-------
10:55
10:56
10:57
10:58
10:59
11:00
11:01
11:02
11:03
11:04
11:05
11:06
11:07
11:08
11:09
11:10
11:11
11:12
11:13
11:14
11:15
11:16
11:17
11:18
11:19
11:20
11:21
Average
Minimum
Maximum
Run 8
M17
Results
Train A
Train B
Average
12.80 15.73
13.01 15.48
11.08 14.28
9.23 17.71
9.35 17.43
10.02 17.80
9.79 14.85
10.27 14.96
10.40 15.04
9.83 14.09
10.34 16.22
8.67 10.51
13.53 24.25
ESC P5B DR 300-40
For P5B &
300-40
mg/acm
22.1
22.14
22.12
10.89
10.17
10.17
10.17
10.17
10.17
10.17
10.17
10.17
10.17
10.17
10.17
10.17
10.17
9.75
9.61
9.61
9.61
9.61
9.61
9.61
9.61
9.61
9.61
9.61
9.61
9.61
9.71
8.90
10.89
F904K
For F904K
&RSD
mg/dscm
33.6
33.7
33.65
14.28
14.28
14.28
14.28
14.28
14.16
14.16
14.04
14.04
14.04
14.23
13.67
14.53
Moisture
Moisture
%
13.8
13.7
13.75
86
86
86
86
86
86
86
86
86
86
85.71
84.00
86.00
Temp
186
24
RCA#1 APPENDIX F
-------
RCA Testing - Run 9: Mid-high PM concentration
8/29/99 ESC P5B Durag 300-40 Durag F904K Moisture
Time raw mA raw ra mA raw mA %
12:05
12:06
12:07
12:08
12:09
12:10
12:11
12:12
12:13
12:14
12:15
12:16
12:17
12:18
12:19
12:20
12:21
12:22
12:23
12:24
12:25
12:26
12:27
12:28
12:29
12:30
12:31
12:32
12:33
12:34
12:35
12:36
12:37
12:38
12:39
12:40
12:41
12:42
12:43
12:44
12:45
12:46
12:47
12:48
12:49
12:50
12:51
12:52
12:53
10.83
9.96
10.35
9.58
10.97
11.22
11.52
11.52
11.29
11.50
11.40
11.05
11.34
11.20
9.08
10.33
10.66
11.11
13.03
13.61
11.53
9.66
9.99
9.84
10.08
10.71
11.06
11.54
10.61
11.71
11.95
11.59
11.84
11.96
11.44
10.22
10.29
11.17
11.49
12.89
13.75
14.18
10.21
10.37
11.42
10.44
11.41
11.60
11.70
18.13
19.62
20.14
18.73
17.56
17.68
17.38
16.30
17.42
18.12
17.40
16.30
16.65
17.05
20.95
22.42
24.58
17.00
16.03
16.32
16.35
18.67
19.81
18.76
16.01
16.98
16.65
16.19
14.10
17.77
18.65
19.02
17.58
18.55
18.75
23.38
27.49
27.40
22.54
17.10
18.38
19.96
18.79
21.91
23.62
17.89
18.21
18.58
, 18.67
10.65
10.41
10.41
10.41
10.41
10.41
10.41
10.41
10.41
10.41
10.41
10.41
10.41
10.89
11.36
11.36
11.36
11.36
11.36
11.36
11.36
11.36
11.36
11.36
11.36
11.36
11.05
10.09
10.09
10.09
10.09
10.09
10.09
10.09
10.09
10.09
10.09
10.09
10.09
14.16
14.16
14.28
14.16
14.28
14.28
14.28
14.28
14.28
14.28
13.79
13.43
13.43
13.67
13.79
14.16
14.28
14.53
14.40
14.16
13.91
14.04
13.91
14.04
14.28
14.28
14.28
14.28
14.28
14.40
14.40
14.28
14.28
14.28
14.28
14.28
14.16
14.16
14.04
14.04
14.04
14.28
14.28
14.28
14.16
13.91
14.04
13.91
13.79
Temp.
degC
86
86
86
86
86
86
86
86
86
86
86
86
86
86
86
86
86
86
86
86
86
86
86
86
86
86
86
86
86
86
86
86
86
86
.86
86
86
86
86
86
86
86
86
86
86
86
86
86
86
25
RCA#1 APPENDIX F
-------
12:54
12:55
12:56
12:57
12:58
13:11
13:12
13:13
13:14
13:15
13:16
13:17
13:18
13:19
13:20
13:21
13:22
13:23
13:24
13:25
13:26
13:27
13:28
13:29
13:30
13:31
13:32
13:33
13:34
13:35
13:36
13:37
13:38
13:39
13:40
13:41
13:42
13:43
13:44
13:45
13:46
13:47
13:48
13:49
13:50
13:51
13:52
13:53
13:54
13:55
13:56
13:57
11.67
12.01
12.15
12.08
12.35
10.49
10.98
11.19
10.01
10.75
10.97
10.19
9.89
10.02
10.39
9.36
10.05
9.57
10.19
12.32
13.25
12.23
9.90
9.86
10.65
10.18
10.68
11.12
10.83
11.02
11.32
11.80
11.16
11.67
11.83
11.76
10.72
10.84
12.02
12.13
14.20
14.72
10.20
10.49
10.64
9.81
10.72
11.25
11.76
11.35
11.84
12.18
17.43
19.06
19.42
17.79
18.24
16.73
16.83
17.45
14.62
15.72
16.24
14.68
14.24
14.94
15.28
18.40
18.83
19.00
14.56
14.27
15.18
15.36
17.71
19.87
21.40
15.60
15.61
16.85
16.54
16.58
17.46
18.72
16.87
17.74
19.48
21.07
26.95
27.46
27.49
16.91
18.59
18.88
18.91
20.50
21.34
19.72
17.56
17.88
19.00
16.23
17.84
18.49
10.09
11.36
11.36
11.36
11.36
11.36
11.36
11.36
11.36
11.36
11.36
11.36
11.36
11.36
11.01
10.33
10.33
10.33
10.33
10.33
10.33
10.33
10.33
10.33
10.33
10.33
10.33
10.41
10.49
10.49
10.49
10.49
10.49
10.49
10.49
10.49
10.49
10.49
10.49
10.49
10.57
10.81
10.81
10.81
10.81
10.81
10.81
10.81
10.81
10.81
10.81
13.79
13.91
13.67
13.50
13.75
13.13
13.26
13.50
13.38
13.38
13.26
12.76
13.01
13.38
13.67
13.79
14.04
14.04
14.16
14.16
14.28
14.28
14.28
14.40
14.28
14.28
14.28
14.16
14.04
14.16
14.16
14.16
13.91
13.91
13.91
14.04
13.91
13.91
13.79
14.04
13.91
14.04
14.04
14.04
13.91
13.79
14.04
14.04
14.04
13.91
14.04
14.04
86
86
86
88
88
88
88
88
88
88
88
88
88
88
86
86
86
86
86
86
86
86
86
86
86
86
86
86
86
86
86
86
86
86
86
86
86
86
86
86
86
86
86
86
86
86
86
86
86
86
86
86
26
RCA#1 APPENDIX F
-------
13:58
13:59
14:00
14:01
14:02
14:03
14:04
14:05
14:06
14:07
14:08
14:09
14:10
14:11
14:12
14:13
11.13
11.54
11.62
11.79
10.27
10.12
10.50
12.31
14.17
14.43
16.98
17.46
18.23
19.63
24.31
26.32
26.14
16.55
18.18
17.90
10.81
10.81
10.81
10.81
10.81
10.81
10.81
10.81
10.81
10.81
10.81
10.81
10.81
10.81
10.81
10.81
13.79
13.91
14.04
14.04
14.04
14.04
14.04
14.16
14.16
14.16
86
86
86
86
86
86
86
86
86
86
Average
Minimum
Maximum
11.23
9.08
14.72
ESC P5B
18.60
14.10
27.49
DR 300-40
10.71
10.09
11.36
F904K
14.01
12.76
14.53
Moisture
Run 9
86.20
86.00
88.00
Temp
187
For P5B &
M17 300-40
Results mg/acm
Train A
Train B
Average
24.17
23.93
24.05
For F904K
&RSD
mg/dscm
36.8
36.4
36.6
Moisture
%
13.9
13.7
13.8
RCA#1 APPENDIX F
27
-------
RCA #1 Testing - Run 10: Mid-high PM concentration
8/29/99 ESC P5B Durag 300-40 Durag F904K Moisture
Time raw mA raw ra mA raw mA %
15:23
15:24
15:25
15:26
15:27
15:28
15:29
15:30
15:31
15:32
15:33
15:34
15:35
15:36
15:37
15:38
15:39
15:40
15:41
15:42
15:43
15:44
15:45
15:46
15:47
15:48
15:49
15:50
15:51
15:52
15:53
15:54
15:55
15:56
15:57
15:58
15:59
16:00
16:01
16:02
16:03
16:04
16:05
16:06
16:07
16:08
16:09
16:10
16:11
10.58
10.78
11.41
10.74
9.60
10.27
10.49
13.15
13.61
14.15
9.52
9.96
10.54
11.04
10.51
11.15
10.90
11.15
11.30
11.69
11.20
11.62
11.37
11.37
10.18
9.83
11.36
12.55
14.66
14.35
10.93
10.11
10.69
11.82
10.91
11.58
12:24
11.56
12.39
12.64
12.48
12.48
12.83
12.94
10.34
10.66
11.30
12.60
14.72
16.44
16.82
17.91
19.51
27.40
26.62
23.14
16.45
18.17
18.32
18.04
21.04
21.55
17.78
17.80
18.28
18.38
16.04
17.42
18.02
17.28
17.75
17.87
19.63
25.93
26.17
25.51
16.04
18.94
19.11
18.70
21.67
22.36
20.68
18.72
19.20
19.48
18.05
19.84
20.74
19.96
19.90
20.77
22.09
31.09
32.26
32.26
21.28
20.80
10.69
11.36
11.36
11.36
11.36
11.36
11.36
11.36
11.36
11.36
11.36
11.36
11.36
11.28
11.05
11.05
11.05
11.05
11.05
11.05
11.05
11.05
1 1 .05
11.05
11.05
11.05
11.05
11.36
11.36
11.36
11.36
11.36
11.36
11.36
11.36
11.36
11.36
11.36
11.36
13.91
14.10
14.16
14.16
14.16
14.16
14.16
14.04
14.16
14.16
14.04
14.04
14.04
14.04
14.16
14.16
14.04
14.04
14.16
14.16
13.79
14.04
13.91
14.04
14.04
14.16
14.16
14.16
14.28
14.40
14.40
14.40
14.28
14.28
14.16
14.16
14.16
14.04
14.16
14.40
14.16
14.40
14.40
14.40
14.40
14.40
14.16
14.04
14.04
Temp.
degC
86
85
86
86
86
86
86
86
86
86
86
86
86
86
86
86
86
86
86
86
86
86
86
86
86
86
86
86
86
86
86
86
86
86
86
86
86
86
86
86
86
86
86
86
86
86
86
86
86
28
RCA#1 APPENDIX F
-------
16:12
16:13
16:14
16:15
16:16
16:17
16:18
16:19
16:20
16:21
16:22
16:23
16:24
16:25
16:26
16:27
16:28
16:29
16:30
16:31
16:32
16:33
16:34
16:35
16:36
16:36
16:38
16:38
16:39
16:40
16:41
16:41
16:42
16:43
16:44
16:45
16:45
16:46
16:47
16:48
16:49
16:50
16:51
16:52
16:53
16:54
16:55
16:56
16:57
16:58
16:59
17:00
14.96
13.35
10.49
11.08
12.66
12.02
12.42
12.76
12.49
13.38
13.41
13.05
12.64
13.01
13.55
10.48
10.89
12.55
11.72
14.96
16.08
15.15
10.24
10.53
11.87
10.44
11.79
11.52
12.89
11.57
12.07
12.22
12.92
13.09
12.35
12.91
12.91
12.98
11.16
11.21
10.60
12.27
15.26
15.12
14.23
10.07
10.91
11.52
10.94
11.69
12.14
11.49
21.79
20.05
23.56
25.69
25.66
21.13
21.88
21.10
20.80
22.09
22.21
22.69
20.08
21.58
22.12
27.76
31.48
31.27
24.52
21.16
21.97
21.22
21.43
23.20
24.70
22.51
19.90
19.54
19.93
18.88
18.91
19.12
21.49
22.48
19.84
21.67
21.49
22.30
27.88
32.14
33.70
23.89
21.19
21.94
21.76
22.27
23.65
24.70
18.97
19.19
19.21
18.76
11.36
12.26
12.56
12.56
12.56
12.56
12.56
12.56
12.56
12.56
12.56
12.56
12.56
12.56
12.56
12.56
12.56
12.56
12.56
12.56
12.56
12.56
12.56
12.56
12.56
12.56
12.56
12.56
12.01
11.45
11.45
11.45
11.45
11.45
11.45
11.45
11.45
11.45
11.45
11.45
11.45
11.45
11.45
11.49
11.61
11.61
11.61
11.61
11.61
11.61
11.61
11.61
14.16
14.27
14.44
14.44
14.44
14.44
14.44
14.44
14.20
14.20
14.27
13.91
13.91
13.91
13.91
13.91
13.79
14.16
14.16
14.16
14.28
14.16
14.16
14.16
14.16
14.16
14.16
14.16
14.28
14.40
14.53
14.53
14.65
14.40
14.40
14.40
14.40
14.28
14.04
13.67
13.67
13.79
13.91
14.16
14.28
14.28
14.28
14.28
14.28
14.28
14.24
14.08
86
86
84
84
84
84
84
84
84
84
86
86
86
86
86
86
86
86
86
86
86
86
86
86
86
86
86
86
86
86
86
86
86
86
86
86
86
86
86
86
86
86
86
86
86
86
86
86
86
86
85
84
29
RCA#1 APPENDIX F
-------
17:01
17:02
17:03
17:04
17:05
17:06
17:07
17:08
17:09
17:10
17:11
17:12
17:13
11:22
11:23
11:24
11:25
11:26
11:27
11:28
11:29
11:30
11:31
11:32
11:33
11:34
11:35
Average
Minimum
Maximum
Run 10
M17
Results
Train A
Train B
Average
11.47 17.33
11.65 18.10
11.91 18.61
10.96 16.79
11.01 17.81
11.63 18.74
10.80 20.80
9.96 27.55
10.93 26.98
11.12 24.25
13.14 17.00
13.81 18.16
14.66 17.79
11.92 21.53
9.52 16.04
16.08 33.70
ESC P5B DR 300-40
For P5B &
300-40
mg/acm
25.94
27.3
26.62
11.61
11.61
11.61
11.61
11.61
11.61
11.61
11.61
11.61
11.61
11.61
11.61
11.61
11.61
11.61
11.61
11.61
11.61
11.42
11.36
11.36
11.36
11.36
11.36
11.36
11.36
11.36
11.36
11.36
11.36
11.36
11.65
10.69
12.56
F904K
For F904K
&RSD
mg/dscm
39.8
42.2
41
14.08
14.08
14.08
13.84
14.08
14.20
14.28
14.28
14.28
14.28
14.16
14.16
14.16
14.18
13.67
14.65
Moisture
Moisture
%
14.2
14.7
14.45
84
84
84
84
84
84
86
86
86
86
86
86
86
85.72
84.00
86.00
Temp
186
30
RCA#1 APPENDIX F
-------
RCA #1 Testing - Run 11: Mid PM concentration
8/30/99 ESC P5B Durag 300-40 Durag F904K Moisture
Time raw mA raw ra mA raw mA %
10:30
10:31
10:32
10:33
10:34
10:35
10:36
10:37
10:38
10:39
10:40
10:41
10:42
10:43
10:44
10:45
10:46
10:47
10:48
10:49
10:50
10:51
10:52
10:53
10:54
10:55
10:56
10:57
10:58
10:59
11:00
11:01
11:02
11:03
11:04
11:05
11:06
11:07
11:08
11:09
11:10
11:11
11:12
11:13
11:14
11:15
11:16
11:17
11:18
9.19
8.68
9.23
9.22
8.74
8.82
8.84
8.72
8.46
9.39
9.03
9.46
10.71
11.03
9.05
8.74
8.72
9.42
9.06
9.63
9.61
8.96
9.40
9.55
9.02
9.03
9.33
9.23
8.12
8.65
9.34
9.53
11.06
11.39
9.75
8.73
8.58
9.77
8.92
9.18
9.46
8.90
9.16
9.19
9.35
8.90
8.40
9.30
8.31
12.74
11.37
12.16
12.44
11.77
12.11
12.99
13.56
15.91
14.52
15.35
10.82
11.40
11.68
11.48
13.37
14.26
13.44
11.85
12.20
12.20
11.74
12.53
12.75
12.29
12.82
13.12
13.73
16.53
18.29
17.12
12.66
12.05 .
12.70
12.13
14.45
14.33
14.69
11.61
11.88
11.97
11.76
11.98
11.89
12.15
11.47
10.72
12.43
14.30
7.78
7.62
7.62
7.62
7.62
7.62
7.62
7.62
7.62
7.62
7.62
7.62
7.62
7.62
7.62
7.62
7.62
7.62
7.62
7.62
7.62
7.62
7.62
7.62
7.62
7.62
7.72
8.02
8.02
8.02
8.02
8.02
8.02
8.02
8.02
8.02
8.02
8.02
8.02
12.16
12.16
12.15
11.97
11.48
11.72
11.85
11.71
11.78
11.91
11.91
12.03
12.03
12.27
12.27
12.40
12.40
12.40
12.52
12.64
12.47
12.45
12.45
12.57
12.21
12.21
12.21
12.21
12.21
12.21
12.21
12.33
12.21
12.33
12.21
12.21
12.33
12.21
12.21
12.21
12.21
12.08
12.08
12.26
12.17
12.26
11.29
11.22
11.98
Temp.
deg C
92
92
92
90
90
90
90
90
88
88
88
88
88
88
88
88
88
88
88
88
87
86
86
86
86
86
86
86
86
86
86
86
86
86
86
86
86
86
86
86
86
86
86
84
85
84
84
86
87
31
RCA#1 APPENDIX F
-------
11:19
11:20
11:21
11:22
11:23
11:24
11:25
11:26
11:27
11:28
11:29
11:30
11:31
11:32
11:33
11:34
11:35
11:36
11:37
11:38
11:39
11:40
11:41
11:42
11:43
11:44
11:45
11:46
11:47
11:48
11:49
11:50
11:51
11:52
11:53
11:54
11:55
11:56
11:57
11:58
11:59
12:00
12:01
12:02
12:03
12:04
12:05
12:06
12:07
12:08
12:09
12:10
8.35
9.16
8.99
11.01
10.88
10.28
8.30
8.64
9.12
8.57
8.94
9.16
8.71
8.91
8.83
8.97
8.42
8.64
8.72
8.35
7.99
8.28
8.86
9.96
10.72
11.07
7.95
8.33
8.41
8.34
8.76
8.95
8.90
7.98
8.80
8.99
8.84
8.45
8.90
8.83
8.40
8.47
8.78
8.93
10.36
10.87
9.60
8.47
8.50
8.36
8.60
8.77
17.38
16.99
13.91
12.20
12.86
12.35
12.58
14.13
14.69
10.86
11.34
11.41
11.46
10.84
11.65
11.80
11.20
11.80
12.27
12.85
16.42
16.03
14.87
11.02
11.37
12.14
11.90
13.10
13.57
11.20
11.05
11.32
11.28
9.65
11.12
11.41
11.14
10.93
11.84
11.75
13.72
16.07
15.60
12.25
11.27
11.51
12.10
12.79
13.38
13.75
11.00
10.97
8.02
7.30
7.30
7.30
7.30
7.30
7.30
7.30
7.30
7.30
7.30
7.30
7.30
7.30
8.33
8.33
8.33
8.33
8.33
8.33
8.33
8.33
8.33
8.33
8.33
8.33
8.33
7.62
7.38
7.38
7.38
7.38
7.38
7.38
7.38
7.38
7.38
7.38
7.38
7.38
7.22
7.05
7.05
7.05
7.05
7.05
7.05
7.05
7.05
7.05
7.05
7.05
11.91
12.03
12.15
12.10
12.21
12.21
11.96
12.33
12.33
12.33
12.45
12.38
12.26
12.26
12.26
12.14
12.02
12.26
12.26
12.14
11.90
12.02
12.02
12.02
12.14
12.02
12.02
12.02
11.77
11.65
11.65
11.77
11.77
12.02
12.50
12.62
12.50
12.62
12.50
12.38
12.14
12.26
12.14
12.26
12.26
12.38
12.38
12.38
12.26
11.90
12.38
12.50
88
88
88
87
86
86
86
86
86
86
86
84
84
84
84
84
84
84
84
84
84
84
84
84
84
84
84
84
84
84
84
84
84
84
84
84
84
84
84
84
84
84
84
84
84
84
84
84
84
84
84
84
32
RCA#1 APPENDIX F
-------
12:11
12:12
12:13
12:14
12:15
12:16
12:17
12:18
12:19
12:20
12:21
12:22
12:23
12:24
12:25
12:26
12:27
12:28
12:29
12:30
12:31
12:32
12:33
12:34
12:35
12:36
12:37
12:38
Average
Minimum
Maximum
Run 11
M17
Results
Train A
Train B
Average
9.22 11.36
8.69 10.27
8.77 10.73
8.79 11.19
9.01 11.53
8.60 10.45
8.78 11.22
8.83 11.52
8.36 11.94
8.76 15.28
9.07 12.62
7.95 9.65
11.39 18.29
ESC P5B DR 300-40
For P5B-&
300-40
mg/acm
12.5
13.44
12.97
7.05
7.21
7.70
7.70
7.70
7.70
7.70
7.70
7.70
7.70
7.70
7.70
7.70
7.70
7.70
7.13
7.13
7.13
7.13
7.13
7.13
7.13
7.13
7.13
7.13
7.13
7.13
7.13
7.57
7.05
8.33
F904K
For F904K
&RSD
mg/dscm
18.7
20.2
19.45
12.50
12.38
12.38
12.50
12.38
12.02
12.38
12.38
12.02
11.90
12.17
11.22
12.64
Moisture
Moisture
%
11.9
12.1
12
84
84
84
84
84
84
84
84
84
84
85.66
84.00
92.00
Temp
186
RCA#1 APPENDIX F
33
-------
RCA #1 Testing - Run 12: Mid-high PM concentration
8/30/99 ESC P5B Durag 300-40 Durag F904K Moisture
Time raw mA raw ra mA raw mA %
13:22
13:23
13:24
13:26
13:27
13:28
13:30
13:31
13:32
13:33
13:34
13:35
13:36
13:37
13:38
13:39
13:40
13:41
13:42
13:43
13:44
13:45
13:46
13:47
13:48
13:49
13:50
13:51
13:52
13:53
13:54
13:55
13:56
13:57
13:58
13:59
14:00
14:01
14:02
14:03
14:04
14:05
14:06
14:07
14:08
14:09
14:10
14:11
14:12
9.74
10.55
12.85
11.06
9.42
9.43
10.15
10.64
10.94
10.02
10.48
10.52
10.63
10.17
10.49
10.31
10.22
9.69
9.95
9.83
12.39
12.31
11.36
9.40
9.83
9.69
9.29
9.93
10.03
9.72
9.64
9.81
10.12
9.72
10.02
9.68
9.66
9.20
9.50
8.94
10.55
11.92
12.44
10.08
9.75
9.55
9.27
9.86
10.13
21.19
14.76
15.32
14.52
17.27
17.94
13.93
14.64
14.80
13.87
14.80
14.88
15.35
13.48
14.51
14.98
16.42
20.29
19.81
15.82
14.64
14.23
14.79
14.77
16.16
16.61
12.46
13.41
13.02
12.76
12.43
13.29
13.72
12.52
13.23
13.52
13.95
17.15
17.60
18.30
11.71
13.31
13.95
13.17
15.63
15.65
13.60
12.57
12.86
9.30
9.30
9.30
9.30
9.30
9.30
9.30
9.30
9.30
9.30
9.30
9.30
9.30
8.18
8.18
8.18
8.18
8.18
8.18
8.18
8.18
8.18
8.18
8.18
8.18
8.18
8.23
8.25
8.25
8.25
8.25
8.25
8.25
8.25
8.25
8.25
8.25
8.25
8.25
8.81
9.37
12.50
12.50
12.50
12.62
12.62
12.62
12.74
12.74
12.74
12.62
12.74
12.87
12.62
12.62
12.62
12.50
12.50
12.50
12.50
12.50
12.50
12.62
12.62
12.62
12.74
12.62
12.62
12.74
12.74
12.74
12.62
12.62
12.26
11.53
11.77
12.02
11.90
11.90
12.02
12.14
12.14
12.50
12.62
12.74
12.74
12.74
12.50
12.50
12.62
Temp.
degC
84
84
84
84
84
84
84
84
84
84
84
84
84
84
84
84
84
84
84
84
84
84
84
84
84
84
84
84
84
84
84
84
84
84
84
84
84
84
84
84
84
84
84
84
84
84
84
84
84
34
RCA#1 APPENDIX F
-------
14:13
14:14
14:15
14:16
14:17
14:18
14:19
14:20
14:21
14:22
14:23
14:24
14:25
14:26
14:27
14:28
14:29
14:30
14:31
14:32
14:33
14:34
14:35
14:36
14:37
14:38
14:39
14:40
14:41
14:42
14:43
14:44
14:45
14:46
14:47
14:48
14:49
14:50
14:51
14:52
14:53
14:54
14:55
14:56
14:57
14:58
14:59
15:00
15:01
15:02
15:03
15:04
10.43
9.02
9.36
9.67
9.74
10.17
9.65
9.90
9.91
10.32
8.97
9.91
9.51
9.89
11.83
12.42
10.63
9.35
9.29
9.12
10.05 .
10.50
10.32
9.97
9.95
10.06
10.52
9.93
9.89
9.96
9.53
9.41
9.54
9.53
11.99
12.13
11.49
9.25
9.50
9.99
9.51
10.15
10.43
10.32
9.64
10.02
10.19
10.20
10.05
10.06
10.41
9.73
13.13
11.62
10.88
11.77
13.68
13.80
12.80
13.39
13.70
14.14
16.42
18.27
18.75
13.10
13.21
13.69
12.83
15.33
15.81
15.15
12.70
12.39
13.32
12.15
13.54
13.96
14.18
12.64
13.53
13.72
14.85
19.30
19.35
15.59
13.73
14.40
14.40
14.66
15.61
15.97
12.71
13.06
13.73
12.82
11.42
13.92
14.16
13.98
13.00
13.57
14.24
16.00
9.37
9.37
9.37
9.37
9.37
9.37
9.37
9.37
9.37
9.37
9.37
9.05
8.10
8.10
8.10
8.10
8.10
8.10
8.10
8.10
8.10
8.10
8.10
8.10
8.10
8.33
8.33
8.33
8.33
8.33
8.33
8.33
8.33
8.33
8.33
8.33
8.33
8.33
8.27
8.25
8.25
8.25
8.25
8.25
8.25
8.25
8.25
8.25
8.25
8.25
8.25
8.14
12.62
12.38
12.38
12.62
12.74
12.74
12.50
12.74
12.74
12.74
12.74
12.62
12.62
12.50
12.62
12.62
12.62
12.62
12.62
12.50
12.74
12.74
12.74
12.62
12.74
12.74
12.74
12.50
12.62
12.62
12.62
12.50
12.62
12.50
12.62
12.50
12.50
12.38
12.38
12.38
12.26
12.50
12.50
12.38
12.38
12.38
12.38
12.14
12.14
12.38
12.38
12.26
84
84
84
84
84
84
84
84
84
84
84
84
84
84
84
84
84
84
84
84
84
84
84
84
84
84
84
84
84
84
84
84
84
84
84
84
84
84
84
84
84
84
84
84
84
84
84
84
84
84
84
84
35
RCA#1 APPENDIX F
-------
15:05
15:06
15:07
15:08
15:09
15:10
15:11
15:12
15:13
15:14
15:15
15:16
15:17
15:18
15:19
15:20
15:21
15:22
15:23
15:24
15:25
15:26
15:27
15:28
15:29
15:30
Average
Minimum
Maximum
Run 12
M17
Results
Train A
Train B
Average
9.96 19.32 8.02 12.26
9.37 19.03 8.02 12.26
9.97 15.17 8.02 12.14
12.30 13.75 8.02 12.14
12.59 14.09 8.02 12.14
11.68 13.53 8.02 12.26
9.43 15.16 8.02 12.38
9.35 16.45 8.02 12.38
8.02
8.02
8.02
8.02
8.04
8.10
8.10
8.10
8.10
8.10
8.10
8.10
8.10
8.10
8.10
8.10
8.10
8.10
10.17 14.59 8.42 12.50
8.94 10.88 8.02 11.53
12.85 21.19 9.37 12.87
ESC P5B DR 300-40 F904K Moisture
For P5B & For F904K
300-40 & RSD Moisture
mg/acm mg/dscm %
18.92 28.4 12.6
19.28 28.9 12.3
19.1 28.65 12.45
84
84
84
84
84
84
84
84
84.00
84.00
84.00
Temp
183
36
RCA#1 APPENDIX F
-------
RCA#1 Appendix G
Statistical Analysis Data and Graphs for PM CEMS
MR1-OPPTR4703-02-07 Appendices Covers WPD
-------
RCA#1 Appendix G1
Statistical Data and Graphs from Initial Correlation
(Linear) and RCA#1 Test Results
MRI-OPPT\R4703-02-07 Appendices Covers. WPD
-------
ESC P5B - Linear
o
35
30
25
y= 1.89X-7.50
20
Emission limit =17 mg/acm
10
12
14
-5
* Init. Corr.
A RCA#1
* 3 MET coal runs
Correlation Line
25% Tl
+ 25% Tl
mA
-------
o
s
w
o
ESC Light Scatter - linear
Run x (mA) y (mg/acm) ylin
17
16
18
21
20
23
13
14
15
19
22
24
1
2
3
4
5
6
7
8
9
10
11
12
5.78
5.87
6
8.97
9.45
9.57
9.6
10.01
10.54
12
13.16
14.5
14.66
6.38
6.41
6.4
8.51
8.35
7.7
10.34
11.23
11.92
9.07
10.17
2.68
3.02
3.2
9.42
10.52
8.755
11.61
13.92
14.46
16.33
15.385
18.655
28.09
1.9
2.54
2.59
9.77
8.29
1 1 .295
22.12
24.05
26.62
12.97
19.1
3.4106
3.5805
3.8260
9.4340
10.3403
10.5669
10.6236
1 1 .3978
12.3985
15.1553
17.3457
19.8759
-------
o
Durag DR 300-40 - Linear
35
30
25
y = 0.71 x-0.82
Emission limit = 17 mg/acm
—i—
12
16
20
24
28
32
-5
* Init. Corr.
A RCA#1
4 3 MET coal runs
Correlation Line
25% Tl
+ 25% Tl
Range Adjusted mA
co
-------
Durag light scatter - linear
Run x (mA) y (mg/acm) ylin
o
16
17
18
21
13
23
20
14
15
19
22
24
1
2
3
4
5
6
7
8
9
10
11
12
6.42
6.44
7.28
14.32
15.45
15.68
15.8
17.22
19.36
20.93
24.54
30.88
28.77
6.11
6.59
6.75
1 1 .72
11.92
10.8
16.22
18.6
21.53
12.62
14.59
3.02
2.68
3.2
9.42
11.61
8.755
10.52
13.92
14.46
16.33
15.385
18.655
28.09
1.9
2.54
2.59
9.77
8.29
1 1 .295
22.12
24.05
26.62
12.97
19.1
3.7340
3.7482
4.3437
9.3348
10.1359
10.2990
10.3841
1 1 .3908
12.9080
14.0210
16.5804
21 .0752
-------
Durag F904K - Linear
o
*d
in
E
o
I
60
50
40
30
y = 3.37x- 12.38
Emission limit = 25.5 mg/dscm
20
10
10
12
14
16
-10
* Init. Corr.
A RCA#1
•» 3 MET coal runs
Correlation Line
+ 25% Tl
mA
-------
Durag Beta Gauge - linear
8.
fc
*""
25
•-d
§
R
O
Run
16
17
18
21
20
23
13
14
15
19
22
24
1
2
3
4
5
6
7
8
9
10
11
12
x (mA)
5.04
5.09
5.21
8.05
8.07
8.08
8.58
9.24
9.98
10.48
10.95
12.57
14.2
5.04
5.07
4.99
7.3
6.99
6.88
9.71
10.71
11.65
7.57
8.42
y (mg/dscm)
4.6
4
4.8
14.3
16.1
13.05
17.2
21.1
21.75
24.4
23.25
28.35
43.05
2.9
3.95
4
14.8
12.65
17.4
33.65
36.6
41
19.45
28.65
ylin
4.6021
4.7706
5.1749
14.7441
14.8115
14.8452
16.5299
18.7537
21.2471
22.9318
24.5154
29.9739
-------
RCA#1 Appendix G2
Statistical Analysis Data and Graphs for PM CEMS
Using Combined Data from Initial Correlation
Tests and RCA #1 Tests
Note: In all statistical tables, Run Numbers 13-24 are from initial correlation tests while Run
Numbers 1-12 are from the RCA tests.
MRJ-OPPT\R4703-02-07 Appendices Covers WPD
-------
o
tr
§. ! g> 5 £>
= £ — £ - Z
1 ^ o o P F
I I
CD
(C
0)
c
13 2
i (0
DQ Q
2 <
o
LU
in
CD
*
\
\
\
\
\
\
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\
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uioe/Buj
RCA#1 APPENDIX G
-------
ESC P5B - Linear
Run
17
16
18
2
4
3
7
6
5
21
11
20
23
13
14
12
8
15
9
10
19
22
24
1
sum
N
xbar
ybar
a
b
R
v (mg/acm)
x (mA) in«i.i con. i RCA« ylin
5.78
5.87
6
6.38
6.4
6.41
7.77
8.35
8.51
8.97
9.07
9.45
9.57
9.6
10.01
10.17
10.34
10.54
11.23
11.92
12
13.16
14.5
14.66
1 1.2069
226.66
24
9.4442
12.3869
2.6170
-12.3290
0.86993
2.68
3.025
3.195
1.895
2.585
2.545
11.295
8.29
9.77
9.415
12.97
10.52
8.755
11.61
13.92
19.1
22.12
14.465
24.05
26.62
16.33
15.385
18.655
28.09
297.285
2.7976
3.0331
3.3733
4.3678
4.4201
4.4463
8.0055
9.5234
9.9421
11.1460
1 1 .4077
12.4021
12.7162
12.7947
13.8677
14.2864
14.7313
15.2547
17.0605
18.8662
19.0756
22.1114
25.6182
26.0370
17
Sxx
Syy
Sxy
f
tf
vf
EL
(x-xbar)A2
13.4261
12.7747
1 1 .8623
9.3891
9.2670
9.2062
2.8028
1.1972
0.8727
0.2248
0.1400
0.0000
0.0158
0.0243
0.3202
0.5268
0.8025
1 .2009
3.1892
6.1298
6.5323
13.8074
25.5615
27.2049
3. 1071874
156.4784
1416.1470
409.5113
22
2.074
1.335
17
(y-ybar)A2 (x-xbar)(y-ybar)
94.2234
87.6447
84.4906
110.0794
96.0768
96.8625
1.1922
16.7844
6.8480
8.8320
0.3400
3.4852
13.1905
0.6035
2.3505
45.0660
94.7337
4.3186
136.0285
202.5818
15.5482
8.9888
39.2894
246.5881
35.5676
33.4609
31.6583
32.1489
29.8385
29.8619
1 .8280
4.4827
2.4446
1.4092
-0.2182
-0.0109
-0.4570
-0.1211
0.8675
4.8726
8.7193
2.2773
20.8284
35.2388
10.0780
11.1405
31.6906
81.9049
SL
Cllow
-0.1323
0.1515
0.5606
1.7511
1.8136
1.8447
6.0024
7.7010
8.1584
9.4422
9.7147
10.7270
11.0390
11.1165
12.1519
12.5449
12.9561
13.4319
15.0163
16.5330
16.7055
19.1536
21.9024
22.2272
14.9645
3.956794
Cl high
5.7275
5.9148
6.1860
6.9845
7.0267
7.0479
10.0086
1 1 .3458
1 1 .7258
12.8497
13.1007
14.0773
14.3933
14.4729
15.5834
16.0279
16.5065
17.0776
19.1046
21.1995
21.4457
25.0692
29.3340
29.8467
19.0355
Cl%
17.2347
16.9509
16.5453
15.3921
15.3329
15.3034
11.7828
10.7202
10.4924
10.0221
9.9589
9.8537
9.8656
9.8720
10.0927
10.2440
10.4425
10.7228
12.0245
13.7251
13.9418
17.3987
21.8576
22.4105
11.9736
nprime
7.8451
8.1100
8.5125
9.8358
9.9119
9.9502
16.7845
20.2768
21.1669
23.2000
23.4955
23.9999
23.9419
23.9109
22.8766
22.2057
21.3697
20.2672
16.1166
12.3701
11.9886
7.6979
4.8775
4.6399
16.2539
un1
1.223
1.223
1.214
1.208
1.208
1.208
1.185
1.179
1.178
1.175
1.175
1.174
1.174
1.174
1.175
1.177
1.178
1.179
1.187
1.199
1.199
1.223
1.266
1.266
1.187
kt
1 .6327
1 .6327
1.6207
1.6127
1.6127
1.6127
1.5820
1.5740
1.5726
1.5686
1.5686
1.5673
1.5673
1 .5673
1 .5686
1.5713
1.5726
1 .5740
1.5846
1.6007
1 .6007
1.6327
1.6901
1.6901
1.5846
Tllow
-3.6627
-3.4272
-3.0394
-2.0132
-1 .9609
-1 .9347
1.7460
3.2955
3.7195
4.9392
5.2009
6.2007
6.5147
6.5933
7.6610
8.0691
8.5087
9.0269
10.7904
12.5327
12.7421
15.6511
18.9308
19.3495
10.7299
Tl high
9.2579
9.4934
9.7861
10.7489
10.8012
10.8274
14.2651
15.7512
16.1647
17.3527
17.6144
18.6036
18.9176
18.9961
20.0744
20.5037
20.9539
21.4826
23.3306
25.1997
25.4091
28.5717
32.3056
32.7244
23.2701
Tl%
38.0016
38.0016
37.7220
37.5355
37.5355
37.5355
36.8209
36.6344
36.6034
36.5102
36.5102
36.4791
36.4791
36.4791
36.5102
36.5723
36.6034
36.6344
36.8830
37.2559
37.2559
38.0016
39.3378
39.3378
36.8830
-------
ESC P5B - Polynomial
All Data
o
£
i
B
O
30
-
JT
y = -27.06 + 5.82x - 0.16xA2
-10
Initial Corr. & RCA#1
•yquad
•Cl low
-Clhigh
--- Tl low
--- Tl high
mA
-------
o
ESC P5B - Polynomial
Run
17
16
18
2
4
3
7
6
5
21
11
20
23
13
14
12
8
15
9
10
19
22
24
1
limit
x(mA)
5.78
5.87
6
6.38
6.4
6.41
7.77
8.35
8.51
8.97
9.07
9.45
9.57
9.6
10.01
10.17
10.34
10.54
11.23
11.92
12
13.16
14.5
14.66
10.85
N
SI
S2
S3
S4
S5
86
S7
DETA
bO
bl
b2
y (mg/acm)
iltlal Corr. ft RCAI
2.68
3.025
3.195
1.895
2.585
2.545
11.295
8.29
9.77
9.415
12.97
10.52
8.755
11.61
13.92
19.1
22.12
14.465
24.05
26.62
16.33
15.385
18.655
28.09
24
226.66
2297.0932
24784.7554
282196.577
297.285
3217.12035
36332.328
4857273.8
-27.06
5.821
-0.162
yquad
1.1646
1.5184
2.0248
3.4736
3.5486
3.5860
8.3741
10.2336
10.7274
12.1007
12.3901
13.4605
13.7888
13.8701
14.9525
15.3601
15.7840
16.2708
17.8506
19.2760
19.4313
21.4494
23.2372
23.4118
(6.9999
X2
33.4084
34.4569
36
40.7044
40.96
41.0881
60.3729
69.7225
72.4201
80.4609
82.2649
89.3025
91.5849
92.16
100.2001
103.4289
106.9156
111.0916
126.1129
142.0864
144
173.1856
210.25
214.9156
117.7246
X3
193.1006
202.262
216
259.6941
262.144
263.3747
469.0974
582.1829
616.2951
721.7343
7461426
843.9086
876.4675
884.736
1003.003
1051.872
1105.507
1170.905
1416.248
1693.67
1728
2279.122
3048.625
3150.663
1277.324
X4
1116.121
1187.278
1296
1656.848
1677.722
1688.232
3644.887
4861.227
5244.671
6473.956
6767.514
7974.937
8387.794
8493.466
10040.06
10697.54
11430.95
12341.34
15904.46
20188.55
20736
29993.25
44205.06
46188.72
13859.09
f 21
sq
Vf
tf
EL
3.844658
1.346
2.08
17
XY
15.4904
17.75675
19.17
12.0901
16.544
16.31345
87.76215
69.2215
83.1427
84.45255
117.6379
99.414
83.78535
111.456
139.3392
194.247
228.7208
152.4611
270.0815
317.3104
195.96
202.4666
270.4975
411.7994
CO
C1
c2
c3
c4
c5
D
X2Y
89.53451
104.2321
115.02
77.13484
105.8816
104.5692
681.9119
577.9995
707.5444
757.5394
1066.976
939.4623
801.8258
1069.978
1394.785
1975.492
2364.973
1606.94
3033.015
3782.34
2351.52
2664.46
3922.214
6036.979
6.9891
•1.4473
0.0702
0.3080
-0.0153
0.0008
4857274
(yhat-y)2
2.2964
2.2698
1.3694
2.4920
0.9285
1.0837
8.5315
3.7776
0.9166
7.2128
0.3363
8.6465
25.3388
5.1081
1.0660
13.9870
40.1443
3.2610
38.4319
53.9341
9.6180
36.7765
20.9968
21.8858
delta
0.2058
0.1907
0.1709
0.1252
0.1232
0.1223
0.0636
0.0641
0.0654
0.0699
0.0709
0.0746
0.0756
0.0758
0.0783
0.0789
0.0794
0.0797
0.0804
0.0858
0.0871
0.1428
0.3716
0.4181
0.0799
sy
r
Cllow
-2.4635
-1.9741
-1.2813
0.6444
0.7415
0.7899
6.3578
8.2083
8.6828
9.9866
10.2604
1 1 .2765
11.5903
1 1 .6683
12.7148
13.1137
13.5312
14.0135
15.5832
16.9339
17.0708
18.4276
18.3622
18.2412
14.7392
7.84676
0.87174
Cl high
4.7927
5.0109
5.3309
6.3028
6.3556
6.3821
10.3904
12.2589
12.7719
14.2148
14.5199
15.6444
15.9872
16.0719
17.1901
17.6065
18.0369
18.5282
20.1181
21.6181
21.7918
24.4711
28.1122
28.5823
19.2606
Cl %
21.3418
20.5439
19.4476
16.6425
16.5121
16.4475
11.8606
11.9136
12.0267
12.4359
12.5280
12.8468
12.9320
12.9519
13.1626
13.2141
13.2521
13.2787
13.3380
13.7769
13.8853
17.7752
28.6765
30.4150
13.2982
n' un'
4.8583 1.266
5.2430 1.266
5.8508 1.247
7.9893 1.223
8.1160 1.223
8.1798 1.223
15.7302 1.187
15.5905
15.2987
14.3082
14.0989
13.4077
13.2316
13.1911
12.7721
12.6726
12.6001
12.5496
12.4384
11.6585
11.4771
7.0035
2.6909
2.3920
12.5129
.187
.189
.192
.192
.195
.195
.195
.195
.195
.195
.195
.199
.199
.203
.233
.340
.433
.195
kt
1.7040
1.7040
1.6785
.6462
.6462
.6462
.5977
.5977
.6004
.6044
.6044
1.6085
1.6085
1.6085
.6085
.6085
.6085
.6085
.6139
.6139
.6192
.6596
.8036
.9288
1.6085
Tllow
-5.3868
-5.0330
-4.4283
-2.8553
-2.7804
-2.7429
2.2315
4.0910
4.5744
5.9322
6.2216
7.2765
7.6047
7.6861
8.7685
9.1761
9.6000
10.0868
11.6459
13.0713
13.2059
15.0687
16.3028
15.9961
10.8159
Tl high
7.7160
8.0698
8.4779
9.8025
9.8775
9.9149
14.5167
16.3762
16.8803
18.2692
18.5586
19.6445
19.9728
20.0541
21.1365
21.5441
21.9681
22.4549
24.0554
25.4807
25.6567
27.8300
30.1716
30.8274
23. 1840
Tl % y-ybar2
38.5379 94.2234
38.5379 87.6447
37.9595 84.4906
37.2289 110.0794
37.2289 96.0768
37.2289 96.8625
36.1330 1.1922
36.1330 16.7844
36.1939 6.8480
36.2853 8.8320
36.2853 0.3400
36.3766 3.4852
36.3766 13.1905
36.3766 0.6035
36.3766 2.3505
36.3766 45.0660
36.3766 94.7337
36.3766 4.3186
36.4983 136.0285
36.4983 202.5818
36.6201 15.5482
37.5333 8.9888
40.7905 39.2894
43.6214 246.5881
36.3766
ybar 12.386875
-------
CD
0)
c
2 «
~ +->
CO =
DC <
O
E
Q
o
cc
r 5 01 5 a
••= £ £ £ - Z
I ^ O O P P
I I
I I
I I
•o
£
"w
3^
1C
0)
D>
C
(0
DC
Luoe/Biu
RCA#1 APPENDIX G
-------
T3
o
Durag
Run
2
16
17
3
4
18
7
5
6
11
21
12
13
23
20
8
14
9
15
19
10
22
1
24
limit
sum
N
xbar
ybar
a
b
R
DR 300-40 -
Linear
v (ma/acm)
X (mA) lilial Corr. & RCAI ylitl
6.11
6.42
6.44
. 6.59
6.75
7.28
10.8
11.72
11.92
12.62
14.32
14.59
15.45
15.68
15.8
16.22
17.22
18.6
19.36
20.93
21.53
24.54
28.77
30.88
19.996
360.54
24
15.0225
12.38688
0.9275
-1.5465
0.824387
1.895
3.025
2.680
2.545
2.585
3.195
11.295
9.770
8.290
12.970
9.415
19.100
11.610
8.755
10.520
22.120
13.920
24.050
14.465
16.330
26.620
15.385
28.090
18.655
297.285
4.1205
4.4081
4.4266
4.5657
4.7141
5.2057
8.4705
9.3238
9.5093
10.1586
1 1 .7353
11.9857
12.7834
12.9967
13.1080
13.4976
14.4251
15.7050
16.4099
17.8661
18.4226
21.2144
25.1377
27.0947
17
Sxx
Syy
Sxy
f
tf
vf
EL
(x-xbar)A2
79.4327
74.0030
73.6593
71.1071
68.4343
59.9463
17.8295
10.9065
9.6255
5.7720
0.4935
0.1871
0.1828
0.4323
0.6045
1.4340
4.8290
12.7985
18.8139
34.8986
42.3476
90.5828
188.9938
251 .4603
24.7379
1118.7747
1416.147
1037.6637
22
2.074
1.335
17
(y-ybar)A2 (x-xbar)(y-ybar)
110.0794
87.6447
94.2234
96.8625
96.0768
84.4906
1.1922
6.8480
16.7844
0.3400
8.8320
45.0660
0.6035
13.1905
3.4852
94.7337
2.3505
136.0285
4.3186
15.5482
202.5818
8.9888
246.5881
39.2894
93.5088
80.5355
83.3093
82.9916
81.0860
71.1681
4.6104
8.6422
12.7106
-1.4010
2.0877
-2.9034
-0.3321
-2.3880
-1.4515
11.6554
3.3690
41.7248
9.0139
23.2940
92.6221
28.5347
215.8787
99.3968
SL
Cl low
0.9591
1.3155
1 .3384
1.5105
1.6938
2.2989
6.2100
7.1881
7.3975
8.1204
9.8026
10.0593
10.8570
11.0652
11.1730
1 1 .5456
12.4054
13.5345
14.1322
15.3237
15.7666
17.9160
20.8154
22.2331
14.6214
4.541294
Cl high
7.2820
7.5007
7.5148
7.6210
7.7345
8.1125
10.7310
11.4595
11.6211
12.1967
13.6680
13.9122
14.7097
14.9282
15.0430
15.4495
16.4448
17.8755
18.6876
20.4084
21.0785
24.5127
29.4600
31.9563
19.3786
Cl %
18.5967
18.1918
18.1658
17.9721
17.7669
17.0989
13.2973
12.5628
12.4221
11.9890
11.3690
11.3319
11.3314
11.3616
11.3823
11.4819
11.8806
12.7677
13.3985
14.9549
15.6233
19.4018
25.4252
28.5977
13.9919
nprime
8.8758
9.2753
9.3018
9.5035
9.7243
10.4988
17.3601
19.4495
19.8925
21.3557
23.7486
23.9041
23.9063
23.7795
23.6928
23.2837
21.7472
18.8301
17.0989
13.7249
12.5757
8.1544
4.7484
3.7533
15.6793
un'
1.214
1.214
1.214
1.208
1.208
1.208
1.185
1.181
.179
.178
.174
.174
.174
.174
1.174
1.175
1.177
1.181
1.185
1.192
1.195
1.223
1.266
1.295
1.187
kt
1 .6207
1 .6207
1.6207
1.6127
1.6127
1.6127
1.5820
1.5766
1.5740
1.5726
1.5673
1 .5673
1 .5673
1.5673
1.5673
1.5686
1.5713
1.5766
1.5820
1.5913
1.5953
1 .6327
1.6901
1.7288
1.5846
Tllow
-3.2395
-2.9520
-2.9334
-2.7579
-2.6095
-2.1179
1.2863
2.1638
2.3615
3.0168
4.6178
4.8682
5.6659
5.8792
5.9905
6.3740
7.2893
8.5450
9.2257
10.6394
11.1777
13.7998
17.4624
19.2436
9.8037
Tl high
11.4806
11.7681
1 1 .7866
11.8894
12.0378
12.5294
15.6547
16.4838
16.6571
17.3003
18.8528
19.1033
19.9009
20.1142
20.2255
20.6211
21.5608
22.8650
23.5941
25.0927
25.6674
28.6290
32.8130
34.9458
24.1963
Tl%
43.2943
43.2943
43.2943
43.0803
43.0803
43.0803
42.2601
42.1174
42.0461
42.0104
41.8678
41.8678
41.8678
41.8678
41.8678
41.9035
41.9748
42.1174
42.2601
42.5097
42.6167
43.6153
45.1487
46.1830
42.3314
-------
o
= >, O O F H
I I
I I
I I
CO
E
o
c
"o
Q.
O =
O <
CO ^
CC
Q
O)
CO
3
D
(0
3^
re
o>
D)
c
re
CC
UJOB/BLU
RCA#1 APPENDIX G
-------
CO
n
I
tfl
o
Durag DR 300-40 -
Run
2
16
17
3
4
18
7
5
6
11
21
12
13
23
20
8
14
9
15
19
10
22
1
24
limit
x(mA)
6.11
6.42
E.44
659
6.75
7.28
108
11.72
11.92
12.62
14.32
14.59
15.45
1568
15.8
1622
17.22
18.6
19.36
20.93
21.53
24.54
28.77
30.88
18.214
N
S1
S2
S3
S4
S5
S6
S7
DETA
bO
bt
b2
Polynomial
y (mg/acm)
Inltui Cotr. 1 RCAIl
1.895
3.025
2.6BO
2.545
2.585
3.195
11.295
9.770
8.290
12970
9.415
19.100
11.610
8.755
10520
22.120
13.920
24050
14.465
16.330
26620
15.385
28.090
18.655
24.000
360.540
6534.987
136093.498
3137877.742
297.285
5503.628
113640.339
1962171830.191
-9.587
2.078
-0.034
yquad
1.8421
2.3544
2.3872
2.6326
2.8926
37415
88956
10.1041
10.3592
11.2307
13.2088
13.5049
14.4151
14.6500
147711
15.1874
16.1304
17.3202
179203
19.0357
19.4179
20.9660
22.1023
22.2151
1 7. oooo
X2
37.3321
41.2164
41.4736
43.4281
45.5625
52.9984
116.6400
137.3584
142.0864
159.2644
205.0624
212.8681
238.7025
245.8624
249.6400
263.0884
296.5264
3459600
374.8096
438.0649
463.5409
602.2116
827.7129
953.5744
331.7325
X3
228.0991
264.6093
2670900
286.1912
307.5469
385.8284
1259.7120
1609.8404
1693.6699
2009.9167
2936.4936
3105.7456
3687.9536
3855.1224
3944.3120
42672938
5106.2190
6434.8560
7256.3139
9168.6984
9980.0356
14778.2727
23813.3001
29446.3775
6042.0192
121
sq 4.1949
vf
II
EL=
1.346
2.08
17
X4 XV X2V
1393.6857 11.5785 70.7443
1698.7916 19.4205 124.6796
17200595 17.2592 111.1492
18B5.9999 16.7716 110.5245
2075.9414 174488 117.7791
2808.6304 23.2596 169.3299
13604.8896 121.9860 1317.4488
18867.3301 114.5044 1341.9916
20188.5451 98.8168 1177.8963
25365.1491 163.6814 2065.6593
42050.5879 134.8228 1930.6625
45312.8280 2786690 40657807
56978.8835 1793745 2771.3360
60448.3197 137.2784 2152.5253
62320.1296 166.2160 2626.2128
69215.5062 358.7664 5819.5154
87929.0920 239.7024 4127.6753
119688.3216 447.3300 8320.3380
140482.2363 280.0424 5421.6209
191900.8566 341.7869 7153.5998
214870.1660 573.1286 12339.4588
3626588112 377.5479 92650255
685108.6448 808.1493 23250.4554
909304.1363 576.0664 17788.9304
f 10046.4743
CO 1.0114045
d -0.123313
c2 0.003241B7
c3 0.01661578
04 -00004638
cS 1.3684E-05
D 1962171830
(yhat-y)2
0.0028
0.4497
0.0857
0.0077
0.0946
0.2986
5.7570
0.1116
4.2816
3.0251
14.3927
31.3053
7.8684
34.7508
18.0720
48.0609
4.8857
45.2902
11.9389
7.321 1
51.8709
31.1476
35.8527
12.6742
delta
0.1743
0.1579
0.1569
0.1496
0.1423
0.1207
0.0598
00586
0.0589
0.0605
0.0679
0.0693
0.0735
0.0745
0.0751
0.0769
0.0805
0.0841
0.0856
0.0891
0.0913
0.1234
0.3201
0.5493
0.0833
sy
r
Cllow
-1.8012
-1.1131
•1.0692
-0.7426
-0.3984
0.7098
6.7628
7.9910
8.2425
9.0848
10.9351
11.2087
12.0501
12.2680
12.3805
12.7681
13.6542
14.7898
15.3676
16.4310
16.7816
17.9013
17.1659
15.7481
14.4824
7.846758
0.845101
Cl high
5.4854
5.8218
5.8436
6.0077
6.1836
6.7731
11.0285
12.2172
12.4760
13.3766
15.4825
15.8011
16.7800
17.0320
17.1618
17.6067
18.6065
19.8506
20.4729
21.6405
22.0541
24.0307
27.0386
28.6821
19.5176
Cl%
21.4311
20.3967
20.3319
19.8537
19.3587
17.8333
12.5461
12.4300
12.4515
12.6229
13.3747
13.5070
13.9114
14.0119
14.0627
14.2309
14.5656
14.8848
15.0155
15.3219
15.5076
18.0275
29.0374
38.0412
14.8092
n'
5.7358
6.3322
6.3726
6.6833
7.0295
8.2835
16.7363
17.0505
16.9916
16.5334
14.7269
14.4398
13.6125
13.4178
13.3210
13.0080
12.4171
11.8903
11.6841
11.2215
10.9544
8.1060
3.1244
1.8204
12.0120
un'
1.247
1.247
1.247
1.233
1.233
1.223
1.185
1.185
1.185
1.185
1.189
1.192
1.192
1.195
1.195
1.195
1.199
1.199
1.199
1.203
1.203
1.223
1.340
1.433
1.199
kt
1.6785
1.6785
1.6785
1.6596
1.6596
1.6462
1.5950
1.5950
1.5950
1.5950
1.6004
1.6044
1.6044
1.6085
1.6085
1.6085
1.6139
1.6139
1.6139
1.6192
1.6192
1.6462
1.8036
1.9288
1.6139
Tllow
-5.1990
-4.6866
-4.6538
-4.3294
-4.0694
-3.1640
2.2047
3.4132
3.6683
4.5398
6.4952
6.7744
7.6846
7.9026
8.0237
8.4400
9.3604
10.5502
11.1503
12.2432
12.6253
14.0605
14.5361
14.1238
10.2300
Tl high
8.8831
9.3954
9.4282
9.5945
9.8546
10.6470
15.5866
16.7951
17.0502
17.9217
19.9223
20.2354
21.1455
21.3974
21.5185
21.9348
22.9004
24.0902
24.6903
25.8283
262104
27.8715
296684
30.3063
23.7700
Tl%
41.4178
41.4178
41.4178
40.9528
40.9528
40.6207
39.3585
39.3585
39.3585
39.3585
394914
39.5910
39.5910
39.6907
39.6907
39.6907
39.8235
39.8235
39.8235
39.9564
39.9564
40.6207
44.5067
47.5956
39.8235
y-ybar2
110.0794
87.6447
94.2234
S6.8625
96.0768
84.4906
1.1922
6.8480
16.7844
0.3400
8.8320
450660
06035
13.1905
34852
94.7337
2.3505
136.0285
4.3186
15,5482
202.5818
8.9888
246.5881
39.2894
ybar 12.387
-------
(0
0)
c
<0
O)
re
<
E
iuosp/6uj
RCA#1 APPENDIX G
-------
Durag F904K - Linear
y (mg/dscm)
Run
4
2
16
3
17
18
7
6
5
11
21
20
23
12
13
14
8
15
19
9
22
10
24
1
sum
N
xbar
ybar
a
b
R
x (mA) initial corr. & RCAti ylin
4.99
5.04
5.04
5.07
5.09
5.21
6.88
6.99
7.3
7.57
8.05
8.07
8.08
8.42
8.58
9.24
9.71
9.98
10.48
10.71
10.95
11.65
12.57
14.2
9.9/767
199.87
24
8.32792
18.7917
4.21973
-16.3499
0.91611
4
2.9
4.6
3.95
4
4.8
17.4
12.65
14.8
19.45
14.3
16.1
13.05
28.65
17.2
21.1
33.65
21.75
24.4
36.6
23.25
41
28.35
43.05
451
4.7065
4.9175
4.9175
5.0441
5.1285
5.6349
12.6818
13.1460
14.4541
15.5935
17.6189
17.7033
17.7455
19.1802
19.8554
22.6404
24.6237
25.7630
27.8729
28.8434
29.8562
32.8100
36.6921
43.5703
25.5
Sxx
Syy
Sxy
f
H
vf
EL
(x-xbar)A2
11.1417
10.8104
10.8104
10.6140
10.4841
9.7214
2.0965
1 .7900
1 .0566
0.5744
0.0772
0.0665
0.0615
0.0085
0.0635
0.8319
1.9102
2.7294
4.6315
5.6743
6.8753
1 1 .0362
17.9953
34.4814
2.5273
155.5422
3300.0633
656.34658
22
2.074
1.335
25.5
(y-ybar)A2 (x-xbar)(y-ybar)
218.7934
252.5451
201.4034
220.2751
218.7934
195.7667
1.9367
37.7201
15.9334
0.4334
20.1751
7.2451
32.9667
97.1867
2.5334
5.3284
220.7701
8.7517
31.4534
317.1367
19.8767
493.2101
91.3617
588.4667
49.3734
52.2505
46.6610
48.3529
47.8942
43.6249
2.0150
8.2170
4.1031
-0.4990
1.2483
0.6942
1 .4235
0.9078
-0.4012
2.1054
20.5355
4.8874
12.0696
42.4209
11.6901
73.7779
40.5472
142.4470
SL
Cllow
1 .2786
1 .5220
1 .5220
1 .6679
1.7651
2.3480
10.2903
10.7976
12.2123
13.4245
15.5278
15.6139
15.6569
17.1001
17.7664
20.4322
22.2583
23.2848
25.1508
25.9965
26.8719
29.3923
32.6522
38.3440
23.0491
4.910359
Cl high
8.1345
8.3131
8.3131
8.4204
8.4919
8.9218
15.0734
15.4944
16.6960
17.7625
19.7101
19.7928
19.8342
21.2604
21.9444
24.8486
26.9891
28.2412
30.5950
31 .6904
32.8404
36.2276
40.7320
48.7965
27.9509
Cl%
13.4429
13.3159
13.3159
13.2401
13.1897
12.8898
9.3785
9.2095
8.7917
8.5058
8.2007
8.1940
8.1908
8.1576
8.1921
8.6596
9.2761
9.7184
10.6748
11.1645
11.7031
13.4026
15.8427
20.4951
9.6112
nprime
8.8263
8.9954
8.9954
9.0987
9.1684
9.6000
18.1340
18.8059
20.6357
22.0460
23.7173
23.7562
23.7745
23.9686
23.7670
21.2698
18.5366
16.8878
13.9972
12.7963
11.6457
8.8794
6.3548
3.7972
17.2667
un' kt
.214 .6207
.214 .6207
.214 .6207
.214 .6207
.214 .6207
1.208 .6127
1.183 1.5793
1.181 1.5766
1.178 1.5726
1.177 1.5713
1.174
1.174
1.174
1.174
.174
.178
.181
.185
.192
.195
.199
.214
.247
1.295
.5673
.5673
.5673
.5673
.5673
.5726
.5766
.5820
.5913
.5953
.6007
.6207
.6647
.7288
1.185 1.5820
Tllow
-3.2516
-3.0406
-3.0406
-2.9140
-2.8296
-2.2839
4.9269
5.4042
6.7320
7.8778
9.9230
10.0074
10.0496
1 1 .4843
12.1594
14.9182
16.8818
17.9950
20.0589
21.0098
21 .9963
24.8518
28.5176
35.081 1
17.7319
Tl high
12.6647
12.8757
12.8757
13.0023
13.0867
13.5537
20.4368
20.8879
22.1763
23.3091
25.3149
25.3993
25.4415
26.8762
27.5513
30.3626
32.3655
33.531 1
35.6868
36.6770
37.7160
40.7681
44.8666
52.0594
33.2681
Tl%
31.2085
31.2085
31.2085
31.2085
31.2085
31.0543
30.4116
30.3602
30.2831
30.2573
30.1802
30.1802
30.1802
30.1802
30.1802
30.2831
30.3602
30.4630
30.6430
30.7201
30.8229
31.2085
32.0568
33.2908
30.4630
-------
(0
"E
o
c
CD
U.
O)
(0
o
CD
O
a:
08
0-0 *£**
.2 § .2 Z .2 3=
1 >; o o F F
v-. *N
\ \
\ \
\ \
\ \
\ \
\ '
\
\
o
in
X
C\S
CD
LO
CO
\
«3
. CM
CO
CD
\
\
. \
O
TT
o
CM
LUOSp/BliJ
RCA#1 APPENDIX G
11
-------
O
tn
o
Durag F904K - Polynomial
Run
4
2
16
3
17
18
7
6
5
11
21
20
23
12
13
14
8
15
19
9
22
10
24
1
limit
x(mA)
4.99
5.04
5.04
5.07
5.09
5.21
6.68
6.99
7.3
7.57
8.05
8.07
8.08
8.42
8.58
9.24
9.71
9.98
10.48
10.71
10.95
11.65
12.57
14.2
9.7624
N
S1
S2
S3
S4
S5
S6
S7
DETA
bO
b1
b2
y (mg/dscm)
Inttkl Corr. 1 RCAIl
4
2.9
4.6
3.95
4
4.8
17.4
1265
148
19.45
14.3
16.1
13.05
28.65
17.2
21.1
33.65
21.75
24.4
36.6
23.25
41
28.35
43.05
24
199.87
1820.0429
17898.6451
187619.6638
451
4412.237
45625.9645
4767289.488
-24.35
6.207
-0.113
yquad
3.8162
4.0700
40700
42220
4.3232
49287
13.0179
13.5287
14.9534
16.1766
183106
18.3984
184422
19.9201
20.6065
233770
25.2901
26.3666
28.3166
29.1947
30.0983
32.6595
35.8576
41.0551
25.5002
X2
24.9001
25.4016
25.4016
25.7049
25.9081
27.1441
47.3344
48.8601
53.2900
57.3049
64.8025
65.1249
65.2864
70.8964
736164
85.3776
94.2841
99.6004
109.8304
114.7041
119.9025
135.7225
158.0049
201 6400
95.3038
\
sq
vf
11
EL
X3
124.2515
128.0241
1280241
130.3238
131.8722
141.4208
3256607
341.5321
389.0170
4337981
521.6601
525.5579
527.5141
596.9477
631.6287
788.8890
915.4986
994.0120
1151.0226
1228.4809
1312.9324
1581.1671
1986.1216
2863.2880
930.3909
21
4.9484
1.346
2.08
25.5
X4 XV X2Y
620.0150 19.9600 99.6004
645.2413 14.6160 73.6646
645.2413 23.1840 116.8474
660.7419 20.0265 101.5344
671.2296 20.3600 103.6324
736.8022 25.0080 130.2917
2240.5454 119.7120 823.6186
2387.3094 88.4235 618.0803
2839.8241 108.0400 788.6920
3283.8516 147.2365 1114.5803
4199.3640 115.1150 926.6758
4241.2526 129.9270 1048.5109
4262.3140 105.4440 851.9875
5026.2995 241.2330 2031.1819
5419.3743 147.5760 1266.2021
7289.3346 194.9640 1801.4674
8889.4915 326.7415 3172.6600
9920.2397 217.0650 2166.3087
12062.7168 255.7120 2679.8618
13157.0306 391.9860 4198.1701
14376.6095 254.5875 2787.7331
18420.5970 477.6500 5564.6225
24965.5484 356.3595 4479.4389
40658.6896 611.3100 8680.6020
9082.8)75
CO 4.4290
01 -1.0327
c2 0.0556
03 0.2497
04 -0.0138
c5 0.0008
D 4767289.4878
(yhat-y)2
0.0338
1.3689
0.2809
0.0740
0.1045
0.0166
19.2026
0.7721
0.0235
10.7154
16.0846
5.2824
29.0760
76.2118
11.6042
5.1849
69.8877
21.3129
15.3401
54.8378
46.8993
69.5640
56.3639
3.9795
delta
0.1621
0.1554
0.1554
0.1515
0.1490
0.1349
0.0621
0.0622
0.0638
0.0663
0.0716
0.0718
0.0720
0.0754
0.0768
0.0804
0.0813
0.0817
0.0836
0.0858
0.0895
0.1140
0.2003
0.6530
0.0814
s
Cllow
•0.3282
0.0123
0.0123
0.2153
0.3500
1.1486
10.4529
10.9618
12.3533
13.5263
15.5559
15.6394
15.6812
17.0931
17.7536
20.4579
22.3553
23.4254
25.3411
26.1807
27.0194
29.1841
31.2516
32.7377
22.5643
y 11.9784
r 0.9107
Cl high
7.9606
8.1276
8.1276
8.2287
8.2965
8.7089
15.5829
16.0955
17.5534
18.8269
21.0652
21.1573
21.2033
22.7470
23.4594
26.2962
28.2250
29.3077
31.2922
32.2088
33.1772
36.1349
40.4636
49.3726
28.4361
Cl%
16.2524
15.9124
15.9124
15.7126
15.5813
14.8241
10.0587
10.0661
10.1962
10.3934
10.8027
10.8193
10.8276
11.0861
11.1878
11.4477
11.5092
11.5339
11.6687
11.8197
12.0741
13.6292
18.0628
32.6175
11.5134
n'
6.1680
6.4344
6.4344
6.5990
6.7107
7.4138
18.1025
16.0787
15.6712
15.0821
139609
13.9180
13.8967
13.2562
13.0164
12.4319
12.2995
12.2468
11.9656
11.6617
11.1756
8.7708
4.9935
1.5314
12.2904
un'
1.247
1.247
1.247
1.233
1.233
1.233
1.187
1.187
1.187
1.189
1.192
1.192
1.192
1.195
1.195
1.199
1.199
1.199
1.199
1.199
1.203
1.214
1.266
1.433
1.199
kt
1.6785
1.6785
1.6785
1.6596
1.6596
1 6596
1.5977
1.5977
1.5977
1.6004
1.6044
1.6044
1 6044
1.6085
1.6085
1.6139
1.6139
1.6139
1.6139
1.6139
1.6192
1.6340
1.7040
1.9288
1.6139
Tl low
-4.4895
•4.2357
•4.2357
-3.9905
-3.8892
•3.2837
5.1118
5.6226
7.0473
8.2572
10.3712
10.4590
105028
11.9607
12.6471
15.3910
17.3041
18.3806
20.3306
21.2087
22.0857
24.5736
27.4253
31.5106
17.5142
Tl high
12.1219
12.3757
12.3757
12.4345
12.5357
13.1412
20.9240
21.4347
22.8594
24.0960
26.2499
26.3377
26.3816
27.8794
28.5659
31.3630
33.2761
34.3526
36.3027
37.1808
38.1110
40.7454
44.2899
50.5997
33.4862
Tl%
32.5714
32.5714
32.5714
32.2057
32.2057
32.2057
31.0042
31.0042
31.0042
31.0565
31.1348
31.1348
31.1348
31.2132
31.2132
31.3177
31.3177
31 3177
31.3177
31.3177
31.4222
31.7095
33.0677
37.4297
31.3177
y-ybar2
218.7934
252.5451
201.4034
220.2751
218.7934
1957667
1 .9367
37.7201
15.9334
0.4334
20.1751
7.2451
32.9667
97.1867
2.5334
5.3284
220.7701
8.7517
31.4534
317.1367
19.8767
493.2101
91.3617
588.4667
ybar 18.7917
-------
Tests for best regression fit
Durag F904K
Polynomial vs. Linear
FfBG
0.66299
Ff (24) = 4.325
less than Ff(24), so linear is better
Durag DR 300-40
Polynomial vs. Linear
Ff DLS 4.782955
greater than Ff(24), so polynomial is better
ESC P5B
Polynomial vs. Linear
Ff ELS 2.302051
less than Ff(24), so linear is better
RCA#1 APPENDIX G
13
-------
RCA No. 1 Appendix G3
Statistical Analysis Data and Graphs for PM CEMS
Using Data only from RCA#1 Tests
MR1-OPPTMU703-02-07 Appendices Covers WPD
-------
ESC P5B - Linear
RCA#1
x»
O
g
%
'-O
£
O
45
40
35
30
25
E
u
15
10 --
-5
y = 3.63x- 19.56
'"*
Emission limit = 1 7 mg/acm
10
mA
12
14
* RCA#1 data
ylin
Cl
Clhigh
Tl low
Tl high
-------
ESC P5B - Linear
y (mg/acm)
Run
2
4
3
7
6
5
11
12
8
9
10
1
limit
sum
N
xbar
ybar
a
b
R
x (mA) RCA#1 data ylin
6.38
6.4
6.41
7.77
8.35
8.51
9.07
10.17
10.34
11.23
11.92
14.66
70.0627
111.21
12
9.2675
14.1108
3.6331
-19.5594
0.955334
1.895
2.585
2.545
11.295
8.29
9.77
12.97
19.1
22.12
24.05
26.62
28.09
169.33
3.6201
3.6928
3.7291
8.6702
10.7774
1 1 .3587
13.3933
17.3897
18.0074
21.2409
23.7478
33.7026
17
Sxx
Syy
Sxy
f
tf
vf
EL
(x-xbar)A2
8.3377
8.2226
8.1653
2.2425
0.8418
0.5738
0.0390
0.8145
1.1503
3.8514
7.0358
29.0791
0.6323813
70.3536
1017.5172
255.6051
10
2.228
1.593
17
(y-ybar)*2 (x-xbar)(y-ybar)
149.2266
132.8448
133.7685
7.9289
33.8821
18.8428
1.3015
24.8918
64.1468
98.7870
156.4793
195.4171
35.2732
33.0503
33.0494
4.2167
5.3406
3.2882
0.2253
4.5027
8.5898
19.5056
33.1806
75.3827
SL
Cllow
0.6362
0.7210
0.7633
6.4158
8.7271
9.3498
11.4696
15.3436
15.9104
18.7729
20.9039
29.0219
14.9819
2.98104
Cl high
6.6041
6.6646
6.6949
10.9246
12.8278
13.3677
15.3170
19.4359
20.1044
23.7089
26.5916
38.3833
19.0181
Cl%
17.5526
17.4813
17.4458
13.2610
12.0608
11.8173
11.3157
12.0363
12.3352
14.5176
16.7287
27.5336
11.8710
nprime
4.9543
4.9948
5.0152
8.6799
10.4933
10.9302
11.9207
10.5362
10.0318
7.2423
5.4544
2.0134
10.8317
un1
1.266
1.266
1.266
1.214
1.208
1.203
1.199
1.203
1.208
1.233
1.266
1.433
1.203
kt
2.0167
2.0167
2.0167
1 .9339
1.9243
1.9164
1.9100
1.9164
1.9243
1.9642
2.0167
2.2828
1.9164
Tllow
-2.3919
-2.3192
-2.2829
2.9052
5.0409
5.6459
7.6995
11.6769
12.2708
15.3856
17.7358
26.8976
1 1.2872
Tl high
9.6321
9.7048
9.7411
14.4352
16.5140
17.0715
19.0871
23.1026
23.7439
27.0962
29.7597
40.5076
22.7128
Tl%
35.3646
35.3646
35.3646
33.9120
33.7444
33.6047
33.4930
33.6047
33.7444
34.4427
35.3646
40.0296
33.6047
-------
W
o
30
E
u
15
10
ESC P5B - Polynomial
RCA#1
y = -46.95 + 9.46x - 0.29xA2
6 ' /
Emission limit = 17 mg/acm
10
mA
12
14
A RCA#1 data
yquad
Cl low
Cl high
Tl low
Tl high
CO
-------
ESC P5B - Polynomial
Run
2
4
3
7
6
5
11
12
a
9
10
1
limit
x(mA)
6.38
6.4
6.41
7.77
8.35
8.51
9.07
10.17
10.34
11.23
11.92
14.66
9.5648
N
S1
S2
S3
S4
S5
S6
S7
DETA
bO
b1
b2
y (mg/acm)
RCAK1 data
1.895
2.585
2.545
1 1 .295
8.29
9.77
12.97
19.1
22.12
24.05
26.62
28.09
12
111.21
1100.9923
11616.8905
129951.307
169.33
1824.8709
20514.8167
455106.36
•46.95
9.460
-0.290
yquad
1.5995
1.7146
1.7720
9.0446
11.8198
12.5510
14.9933
19.2612
19.8581
22.7097
24.6043
29.4018
17.0001
X2 X3
40.7044 259.6941
40.96 262.144
41.0BB1 263.3747
60.3729 469.0974
69.7225 582.1829
72.4201 616.2951
82.2649 746.1426
103.4289 1051.872
106.9156 1105.507
126.1129 1416.248
142.0864 1693.67
214.9156 3150.663
91.48809 875.0494
f 9
sq 2.198893
vf 1.645
K 2.262
EL 17
X4
1656.848
1677.722
1688.232
3644.887
4861.227
5244.671
6767.514
10697.54
11430.95
15904.46
20188.55
46188.72
8369.704
XY
12.0901
16.544
16.31345
87.76215
69.2215
83.1427
117.6379
194.247
228.7208
270.0815
317.3104
411.7994
CO
C1
C2
C3
c4
c5
D
X2Y
77.13484
105.8816
104.5692
681.9119
577.9995
707.5444
1066.976
1975.492
2364.973
3033.015
3782.34
6036.979
17.8491
-3.6514
0.1752
0.7630
-0.0373
0.0019
455106.4
(yhat-y)2
0.0873
0.7576
0.5975
5.0643
12.4593
7.7339
4.0939
0.0260
5.1161
1.7963
4.0630
1.7209
delta
0.2919
0.2865
0.2839
0.1183
0.1193
0.1228
0.1403
0.1721
0.1752
0.1857
0.1995
0.9045
0. 1567
sy
r
Cllow
•1 .0877
-0.9477
-0.8780
7.3338
10.1021
10.8078
13.1300
17.1975
17.7761
20.5666
22.3826
24.6714
(5.0308
9.61777
0.97351
Cl high
4.2867
4.3769
4.4220
10.7553
13.5374
14.2942
16.8567
21.3248
21.9401
24.8528
26.8260
34.1323
18.9693
Cl%
15.8069
15.6606
15.5882
10.0633
10.1039
10.2544
10.9608
12.1391
12.2470
12.6066
13.0689
27.8264
1 1.5838
n'
3.4261
3.4904
3.5229
8.4532
8.3853
8.1410
7.1255
5.8093
5.7073
5.3864
5.0121
1.1056
6.3796
un'
1.340
1.340
1.295
1.223
1.223
1.223
1.233
1.247
1.247
1.266
1.266
1.433
1.247
kt
2.2043
2.2043
2.1303
2.0118
2.0118
2.0118
2.0283
2.0513
2.0513
2.0826
2.0826
2.3573
2.0513
Tllow
-3.2475
-3.1324
-2.9122
4.6208
7.3960
8.1272
10.5334
14.7506
15.3475
18.1304
20.0250
24.2184
12.4895
Tl high
6.4465
6.5618
6.4563
13.4684
16.2436
16.9748
19.4533
23.7718
24.3688
27.2891
29.1837
34.5853
21.5107
Tl%
28.5119
28.5119
27.5544
26.0224
26.0224
26.0224
26.2352
26.5331
26.5331
26.9373
26.9373
30.4907
26.533 f
y-ybar2
149.2266
132.8448
133.7685
7.9289
33.8821
18.8428
1.3015
24.8918
64.1468
98.7870
156.4793
195.4171
ybar
14.1108333
Q
-------
'-a
frl
O
45
40
35
30
25
o
"6>
20
15
10
-5
Durag DR 300-40 - Linear
RCA#1
y=1.35x-4.61
Emission limit = 17 mg/acm
12
16
20
24
28
* RCA#1 data
Cl
Cl high
Tl low
Tl high
Range adjusted mA
-------
Durag
Run
2
3
4
7
5
6
11
12
8
9
10
1
limit
sum
N
xbar
ybar
a
b
R
DR 300-40
x(mA)
6.11
6.59
6.75
10.8
11.72
11.92
12.62
14.59
16.22
18.6
21.53
28.77
15.990
166.22
12
13.85167
14.11083
1.351185
-4.60533
0.939963
- Linear
y (mg/acm)
RCA#1 data
1.895
2.545
2.585
1 1 .295
9.77
8.29
12.97
19.1
22.12
24.05
26.62
28.09
169.33
ylin
3.6504
4.2990
4.5152
9.9875
1 1 .2306
11.5008
12.4466
15.1085
17.3109
20.5267
24.4857
34.2683
17
Sxx
Syy
Sxy
f
tf
vf
EL
(x-xbar)A2
59.9334
52.7318
50.4337
9.3127
4.5440
3.7313
1.5170
0.5451
5.6090
22.5467
58.9568
222.5567
4.5721
492.41817
1017.5172
665.34793
10
2.228
1.593
17
(y-ybar)A2
149.2266
133.7685
132.8448
7.9289
18.8428
33.8821
1.3015
24.8918
64.1468
98.7870
156.4793
195.4171
(x-xbar)(y-ybar)
94.5709
83.9872
81.8526
8.5930
9.2532
11.2439
1.4051
3.6837
18.9684
47.1945
96.0496
208.5459
SL
Cllow
0.1773
0.9520
1.2095
7.5349
8.8971
9.1882
10.1920
12.8797
14.9503
17.7706
21.0294
28.6566
14.6658
3.442516
Cl high
7.1235
7.6459
7.8208
12.4400
13.5640
13.8134
14.7013
17.3372
19.6715
23.2828
27.9419
39.8799
19.3342
Cl%
20.4300
19.6879
19.4451
14.4266
13.7264
13.6035
13.2628
13.1104
13.8858
16.2122
20.3309
33.0097
13.7306
nprlme
4.8770
5.2515
5.3835
9.7804
10.8037
10.9998
11.5722
11.8427
10.5570
7.7447
4.9246
1.8681
10.7970
un'
1.266
1.266
1.266
1.208
1.203
1.203
1.199
1.199
1.203
1.223
1.266
1.433
1.203
kt
2.0167
2.0167
2.0167
1.9243
1.9164
1.9164
1.9100
1.9100
1.9164
1.9482
2.0167
2.2828
1.9164
Tl low
-3.2922
-2.6437
-2.4275
3.3629
4.6334
4.9036
5.8714
8.5332
10.7137
13.8199
17.5430
26.4098
10.4028
Tl high
10.5931
11.2416
1 1 .4578
16.6121
17.8277
18.0980
19.0219
21.6837
23.9081
27.2336
31.4283
42.1267
23.5972
Tl%
40.8391
40.8391
40.8391
38.9682
38.8069
38.8069
38.6778
38.6778
38.8069
39.4520
40.8391
46.2263
38.8069
-------
03
T3
O
DC
-
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s g>
F F
I I
I I
I I
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o
c
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o
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6
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o
DC
Q
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£
3
Q
in
CO
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\ \
\
\
\
CvJ
X
LO
O
X
q
cd
CC)
o
CD
\
\
\
\
\
C
o
'to
to
UJ
\
\
\
co
CM
CM
0
CM
CO
•o
(U
(0
(U
D>
C
(0
oc
CM
\
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\
\
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in
CM
o
CM
in o
IUOE/6UI
in
RCA#1 APPENDIX G
-------
oo
Durag DR 300-40 - Polynomial
y (mg/acm)
Run x (mA) RCAffl data
2 6.11 1895
3 6.59 2.545
4 6.75 2.585
7 10.8 11295
5 11.72 9.77
6 11.92 8.29
11 12.62 12.97
12 14.59 19.1
8 16.22 22.12
9 186 24.05
10 21.53 26.62
1 28.77 28.09
limit 14.348
N
S1
S2
S3
S4
S5
86
S7
DETA
bO
b1
b2
12
166.22
2794.8422
54996.2074
1217577.01
169.33
3010.85065
59997.592
166708630
-16.11
3.040
-0.051
yquad
0.5635
1.7115
2.0889
10.7718
12.5106
12.8772
14.1279
17.3793
19.7697
22.7724
25.6742
29.0830
17.0005
X2 X3
37.3321 228.0991
43.4281 286.1912
45.5625 307.5469
116.6400 1259.7120
137.3584 1609.8404
142.0864 16936699
159.2644 20099167
212.8681 3105.7456
263.0884 4267.2938
345.9600 64348560
463.5409 9980.0356
827.7129 23813.3001
2058512 2953.4526
f a
i y
sq 2.2331
vf 1645
tf 2.262
EL= 17
X4 XY X2Y (yhat-y)2
1393.6857 11.5785 70.7443 1.7729
1885.9999 16.7716 110.5245 0.6947
2075.9414 17.4488 117.7791 0.2461
13604.8896 121.9860 1317.4488 0.2737
18867.3301 114.5044 1341.9916 7.5109
20188.5451 98.8168 1177.8963 21.0421
25365.1491 163.6814 2065.6593 1.3408
45312,8280 2786690 4065.7807 2.9609
692155062 358.7864 5819.5154 5.5241
119688.3216 447.3300 8320.3380 1.6323
214870.1660 573.1286 12339.4588 0.8945
6851086448 808.1493 23250.4554 0.9861
42374.7041
CO 2.26954523
c1 -0.2920061
C2 0.00797995
C3 0.04078842
c4 -0.0011721
c5 3.5445E-05
D 166708630
delta
0.3345
0.2813
0.2657
0.1106
0.1148
0.1166
0.1248
0.1545
0.1768
0.1976
0.2222
0.9005
0. 1507
sy
r
Cllow
-2.3578
•0.9678
-0.5148
9.0919
10.7990
11.1521
12.3435
15.3940
17.6456
20.5270
23.2929
24.2898
(5.0393
9.617773
0.972673
Cl high
3.4847
4.3908
4.6926
12.4516
14.2222
14.6023
159124
19.3645
21.8938
25.0178
28.0555
338762
18.9616
17.1838
15.7604
15.3159
9.8815
10.0680
10.1477
10.4969
11.6781
12.4947
13.2085
14.0076
28.1953
11.5363
n'
2.9899
3.5543
3.7636
9.0416
8.7097
8.5734
80124
6.4736
5.6551
5.0604
4.4995
1.1105
6.6337
un'
1.340
1.295
1.295
1.214
1.214
1.214
1.223
1.247
1.247
1.266
1.295
1.433
(.233
kt
2.2043
2.1303
2.1303
1 .9970
1.9970
1 .9970
2.0118
2.0513
2.0513
2.0826
2.1303
2.3573
2.0283
Tllow
-4.3588
-3.0455
-2.6681
6.3123
8.0511
8.4177
9.6354
12.7985
15.1890
18.1219
20.9172
23.8191
12.4712
Tl high
5.4858
6.4685
6.8460
15.2313
16.9701
17.3367
186205
21.9600
24.3504
27.4229
30.4313
34.3470
21.5297
289550
27.9826
27.9826
26.2323
26.2323
26.2323
26.4268
26.9454
26.9454
27.3559
27.9826
30.9645
26.6429
y-ybar2
149.2266
133.7685
132.8448
7.9289
18.8428
33.8821
1.3015
24.6918
64.1468
98.7870
156.4793
195.4171
ybar
14.1108333
tn
Q
-------
0
'-a
fl
Q
70
60
50
40
30
20
10
-10
Durag F904K - Linear
RCA#1
= 4.92x- 18.88
..'"•
Emission limit = 25.5 mg/dscm
10
mA
12
14
RCA#1 data
-ylin
-Cl
•Clhigh
Tl low
Tl high
-------
Durag F904K - Linear
Run
4
2
3
7
6
5
11
12
8
9
10
1
limit
sum
N
xbar
ybar
a
b
R
x(mA)
4.99
5.04
5.07
6.88
6.99
7.3
7.57
8.42
9.71
10.71
11.65
14.2
9.02241
98.53
12
8.21083
21 .5083
4.91838
-18.8757
0.96273
y (mg/dscm)
RCA#1 data
4
2.9
3.95
17.4
12.65
14.8
19.45
28.65
33.65
36.6
41
43.05
258.1
ylin
5.6670
5.9130
6.0605
14.9628
15.5038
17.0285
18.3565
22.5371
28.8818
33.8002
38.4235
50.9654
25.5
Sxx
Syy
Sxy
tf
vf
EL
(x-xbar)A2
10.3738
10.0542
9.8648
1.7711
1 .4904
0.8296
0.4107
0.0438
2.2475
6.2458
11.8279
35.8701
0.6587
91 .029692
2375.8442
447.71892
10
2.228
1.593
25.5
(y-ybar)-2
306.5417
346.2701
308.2951
16.8784
78.4701
45.0017
4.2367
51.0034
147.4201
227.7584
379.9251
464.0434
(x-xbar)(y-ybar)
56.3914
59.0039
55.1478
5.4675
10.8145
6.1102
1.3190
1 .4938
18.2024
37.7166
67.0351
129.0166
SL
Cllow
1.5415
1.8242
1.9938
1 1 .9849
12.5710
14.2044
15.6036
19.8481
25.8291
30.1796
34.1341
44.5479
22.7048
4.168824
Cl high
9.7926
10.0017
10.1272
17.9406
18.4367
19.8526
21.1093
25.2261
31 .9345
37.4207
42.7128
57.3828
28.2952
16.1788
16.0342
15.9479
11.6779
11.5014
11.0748
10.7956
10.5450
11.9715
14.1982
16.8210
25.1664
10.9617
nprime
5.0686
5.1604
5.2164
9.7286
10.0294
10.8170
11.3837
11.9312
9.2573
6.5813
4.6889
2.0948
11.0413
un'
1.266
1.266
1.266
1.208
1.208
1.203
1.203
1.199
1.214
1.233
1.266
1.433
1.203
kt
2.0167
2.0167
2.0167
1.9243
1.9243
1.9164
1.9164
1.9100
1 .9339
1.9642
2.0167
2.2828
1.9164
Tl low
-2.7404
-2.4945
-2.3469
6.9405
7.4816
9.0395
10.3674
14.5746
20.8197
25.6119
30.0160
41.4489
17.5110
Tl high Tl %
14.0745 32.9703
14.3204 32.9703
14.4679 32.9703
22.9850 31.4598
23.5261 31.4598
25.0176 31.3296
26.3455 31.3296
30.4996 31.2254
36.9439 31.6161
41.9885 32.1109
46.8309 32.9703
60.4818 37.3195
33.4890 31.3296
-------
E
o
c
_>
o
ft ^~
O)
LL
O)
utosp/Bui
RCA#1 APPENDIX G
11
-------
to
Durag F904K - Polynomial
Run
4
2
3
7
6
5
11
12
8
9
10
1
limit
x(mA)
499
5.04
5.07
6.88
6.99
7.3
7.57
8.42
9.71
10.71
11.65
14.2
840(6
N
S1
S2
S3
S4
S5
S6
S7
DETA
bO
b1
b2
y (mg/dscm)
RCAH1 data
4
2.9
3.95
17.4
12.65
14.8
19.45
2865
33.65
36.6
41
43.05
12
98.53
900.0431
9057.9896
98829.6368
2581
2566.935
27267.0069
833950.6757
-48.00
1 1 .992
-0.386
yquad
2.2274
2.6334
2.8760
16.2310
16.9611
18.9683
20.6562
25.6021
32.0427
36.1513
39.3094
44.4411
25.5007
X2
24.9001
25.4016
25.7049
47.3344
488601
53.2900
57.3049
70.8964
942841
114.7041
135.7225
201.6400
70.5860
1
sq
vf
It
EL
X3 X4 XY X2Y
124.2515 620.0150 19.9600 99.6004
128.0241 645.2413 14.6160 736646
1303238 660.7419 20.0265 101.5344
325.6607 2240.5454 119.7120 823.6186
341 5321 2387.3094 88.4235 618.0803
3890170 2839.8241 108.0400 788.6920
4337981 3283.8516 147.2365 1114.5803
5969477 5026.2995 241.2330 2031.1819
9154986 8889.4915 326.7415 3172.6600
12284809 131570306 391.9860 4198.1701
1581 1671 18420.5970 477.6500 5564.6225
2863.2880 40658.6896 611.3100 8680.6020
593.0322 4982.3894
g cO 8.2784
cl -1.9007
2 5823 C2 0.0988
C3 0.4507
1 645 c4 -0.0240
2262 c5 0.0013
0 833950.6757
25.5
(yhat-y)2
3.1421
0.0711
1.1534
1 .3666
18.5853
17.3750
1.4548
9.2895
2.5835
0.2013
28580
1.9352
delta
0.3013
0.2883
0.2808
0.1169
0.1184
0.1255
0.1343
0.1664
0.1958
0.2005
0.2202
0.8515
0.1657
Cllow
•0.9788
•0.5031
-0.2195
14.2336
14.9514
16.8989
18.5153
23.2195
29.4577
33.5356
36.5686
39.0510
23. 1228
Cl high
5.4336
5.7698
5.9715
18.2283
18.9707
21.0378
22.7970
27.9848
34.6276
38.7671
42.0503
49.8312
27.8787
12.5733
12.2998
12.1392
7.8328
7.8811
8.1156
8.3955
9.3437
10.1371
10.2578
10.7483
21.1377
9.3253
n
3.3192
3.4684
3.5608
8.5525
8.4480
7.9668
7.4445
6.0102
5.1063
4.9867
4.5420
1.1744
6.0340
1.340
1.340
1.295
1.214
1.223
1 223
1.233
1.247
1.266
1.266
1.266
1.433
1.247
kt
2.2043
2.2043
2.1303
1 .9970
2.0118
2.0118
2.0283
2.0513
2.0826
2.0826
2.0826
2.3573
2.05(3
Tllow
-3.4648
-3.0589
-2.6250
1 1 .0740
11.7658
13.7731
15.4185
20.3050
26.6648
30.7734
33.9316
38.3538
20.2035
Tl high
7.9196
8.3256
8.3771
21.3880
22.1563
24.1636
25.8939
30.8993
37.4206
41.5292
44.6873
50.5284
30.7979
Tl % y-ybar2
22.7689 306.5417
22.7689 346.2701
22.0043 308.2951
20.6280 16.8784
20.7809 784701
20.7809 45.0017
20.9508 4.2367
21.1887 51.0034
21.5115 147.4201
21.5115 227.7584
21.5115 379.9251
24.3491 464.0434
21.1687
sy 14.6965
f 0.9844
ybaf
21.5083
o
-------
Tests for best regression fit
Durag F904K
Polynomial vs. Linear
FfBG
17.06177
(12) =
5.12
greater than Ff(12), so polynomial is better
Durag DR 300-40
Polynomial vs. Linear
Ff DLS 14.76566
greater than Ff(12), so polynomial is better
ESC P5B
Polynomial vs. Linear
R ELS 9.379223
greater than Ff(12), so polynomial is better
RCA#1 APPENDIX G
13
-------
1. REPORT NO.
EPA-454/R-00-040C
TECHNICAL REPORT DATA
(Please read Instructions on reverse before completing)
3. RECIPIENT'S ACCESSION NO.
4. TITLE AND SUBTITLE
5. REPORT DATE September 2000
6. PERFORMING ORGANIZATION CODE
7. AUTHOR(S) Dan Bivins
Emission Monitoring and Analysis Division
?. PERFORMING ORGANIZATION NAME AND ADDRESS
U.S. Environmental Protection Agency
Office of Air Quality Planning and Standards
Research Triangle Park, NC 27711
2. SPONSORING AGENCY NAME AND ADDRESS
Director
Office of Air Quality Planning and Standards
Office of Air and Radiation
U.S. Environmental Protection Agency
Research Triangle Park, NC 27711
5. SUPPLEMENTARY NOTES
8. PERFORMING ORGANIZATION REPORT NO.
10. PROGRAM ELEMENT NO.
11. CONTRACT/GRANT NO.
68-D-98-027
13. TYPE OF REPORT AND PERIOD COVERED
Final
14. SPONSORING AGENCY CODE
EPA/200/04
5. ABSTRACT " ~~
'his final report describes an extended field demonstration of three paniculate matter (PM) continuous
mission monitoring systems (CEMS) at a coal-fired boiler equipped with a lime slurry scrubber™
fePMCEM^n^011 T^'^ ^^ °bJ'ectives of *« field stlidy ^ere to: (1) demonstrate whether
ic PM CEMS could provide reliable and accurate data over an extended period, (2) evaluate the PM CEMS
™T * «' d a*1*1 setup/maintenance requirements, and (3) determine whether the PM
EMS satisfy all the requirements of draft PS-11 and the quality assurance (QA) criteria specified in draft
rocedure 2, or determine if changes are needed in the requirements of PS-11 Jd/or Procetoe 2 That
-port presents the results of the study involving two different PM CEMS technologies (light scatter and beta
auge) at the coal-fired boiler. The report consists of five separate volumes.
KEY WORDS AND DOCUMENT ANALYSIS
DESCRIPTORS
-11
;tbod 17
ocedure 2
}isture CEMS
•monstration
rticulate Matter
t CEMS
DISTRIBUTION STATEMENT
Release Unlimited
b. IDENTIFIERS/OPEN ENDED TERMS
Air Pollution control
19. SECURITY CLASS (Report)
Unclassified
20. SECURITY CLASS (Page)
Unclassified
Form 2220-1 (Rev. 4-77) PREVIOUS EDITION IS OBSOLETE
c. COSATI Field/Group
21. NO. OF PAGES
290
22. PRICE
-------