United States
       Environmental Protection
       Agency
Office of Air Quality
Planning and Standards
Research Triangle Park, NC 27711
EPA-454/R-00-040d
September 2000
      Air
      EVALUATION OF PARTICULATE MATTER
E PA  (PM) CONTINUOUS EMISSION
      MONITORING SYSTEMS (CEMS)
      Final Report
      Volume 4 — Appendices for RCA No. 2

-------
                             Volume 4—Appendices for RCA No.  2
                                       Table of Contents

          RCA #2 Appendix A—Process Operating Conditions
          RCA #2 Appendix B—Computer Results for M17 Tests
          RCA #2 Appendix C—M17 Field Sampling Data Sheets
          RCA #2 Appendix D—M17 Field Laboratory Particulate Weight Data
          RCA #2 Appendix E—M17 Post-Test Calibration Sheets
          RCA #2 Appendix F—PM CEMS Data for Each Run
          RCA #2 Appendix G—Statistical Analysis Data and Graphs from Initial Correlation
                                    and RCA Data
-
*
                                        U S Environmental Protection Agency
                                        Region 5, Library (PL-12J)
                                        77 West Jackson Boulevard, 12tn Floor
                                        Chicago, 11  60604-3590

-------
                                RCA #2 Appendix A
                      Process Operating Conditions
MRJ-OPPT\R4703-02-07 Appendices Covers WPD

-------
                       Time
                  Parameters
           Steam Flow (klb/hr)
          Steam Temp (deg F)
              Coal Row (Ib/hr)
              Boiler O2s (Avg)
                        west
                      central
                        east
 East Undergrate Air Flow (Ib/hr)
West Undergrate Air Flow (Ib/hr)
   Baghouse Inlet Temp (deg F)
 Baghouse Outlet Temp (deg F)
        Baghouse DP (in H20)
   ID Fan Suet. Press, (in H2O)
   2A SDA Outlet Temp (deg F)
        2A Atomizer KW (KW)
              U2 % Solids (%)
           2A Lime Flow (gpm)
                     Opacity
                       Time
                  Parameters
           Steam Flow (klb/hr)
          Steam Temp (deg F)
              Coal Flow (Ib/hr)
              Boiler O2s (Avg)
                        west
                      central
                        east
 East Undergrate Air Flow (Ib/hr)
West Undergrate Air Flow (Ib/hr)
   Baghouse Inlet Temp (deg F)
 Baghouse Outlet Temp (deg F)
        Baghouse DP (in H2O)
   ID Fan Suet. Press, (in H2O)
   2A SDA Outlet Temp (deg F)
        2A Atomizer KW (KW)
              U2 % Solids (%)
          2A Lime Row (gpm)
                     Opacity
Run #30
12:15
I
275.9
963
30857
2.7
: 3.6
3
: 1.5
133341
130948
185.9
171.5
10
-25.5
185.6
66
35.6
2.6
8.40
Run #31


















12:30
276.2
961
36000
2.8
3.7
2.8
1.8
130438
133543
186.3
172.9
9.7
-24.9
185.9
66
35.6
2.3


15:45
271.7
945
27000
2.9
4.8
2.8
1.2
131457
132528
185.2
174.1
10.3
-25.5
185
66
33.8
5
12:45
275.3
963
28421
2.6
3.6
2.5
1.7
130182
130029
184.7
173.6
10
-25.4
183.4
67
35.3
5.3


16:00
266.1
945
26341
3.1
5.5
2.4
1.5
129271
128296
185.4
174.3
9.8
-25.4
182.4
68
35.7
5.2
13:00
279.6
959
15652
2.4
3.4
2.3
1.4
130598
130059
186.3
173.7
10
-19.6
186.3
65
35.4
3.9


16:15
267.4
942
28421
2.9
5.3
2.6
0.8
128952
131384
184.9
173.7
10
-25.5
190
65
35
2.1
13:15
277.5
960
27000
2.4
3.6
2.5
1.1
127862
132575
183.8
176.6
9.8
-25.3
186.5
65
35.2
3.3


16:30
269.2
948
30000
3.2
5.6
3.4
0.5
127955
132474
183.7
173.7
9.7
-25.4
190
63
35.3
4.7
13:30
273.8
952
27692
2.5
3.5
2.5
1.5
130396
129388
185.4
175
10.3
-25.5
184
66
34.8
4.3


16:45
271.3
947
26341
3.1
5.4
3.4
0.4
131841
130199
186.4
174.8
11
-25.8
197
58
35
5.4
13:45
276.4
961
27692
2.4
3.2
2.4
1.6
130294
129878
187.3
175.5
10.1
-25.2
181.1
70
35
3.6




















14:00
273.9
967
28421
2.5
3.6
2.4
1.5
129859
129698
187.2
175.6
10.4
-25.6
187.1
67
37.2
3.1




















                                                                                       Run #30 Avg
                                                            276.1
                                                             961
                                                            27717
                                                             2.5
                                                             3.5
                                                             2.6
                                                             1.5
                                                           130371.3
                                                           130764.8
                                                            185.9
                                                            174.3
                                                             10.0
                                                            -24.6
                                                            185.0
                                                             66.5
                                                             35.5
                                                             3.6
                                                                                       Run #31 Avg
                                                            269.1
                                                            945.4
                                                           27620.6
                                                             3.0
                                                             5.3
                                                             2.9
                                                             0.9
                                                           129895.2
                                                           130976.2
                                                            185.1
                                                            174.1
                                                             10.2
                                                            -25.5
                                                            188.9
                                                             64.0
                                                             35.0
                                                             4.5
8.67
                                   RCA#2 APPENDIX A

-------
                            Run #32
                       Time  9:00   9:15
                  Parameters
           Steam Flow (klb/hr)
          Steam Temp (deg F)
              Coal Flow (Ib/hr)
              Boiler 02s (Avg)
                        west
                      central
                        east
 East Undergrate Air Flow (Ib/hr)
West Undergrate Air Flow (Ib/hr)
   Baghouse Inlet Temp (deg F)
 Baghouse Outlet Temp (deg F)
        Baghouse DP (in H2O)
   ID Fan Suet. Press, (in H2O)
   2A SDA Outlet Temp (deg F)
        2A Atomizer KW (KW)
              U2 % Solids (%)
          2A Lime Flow (gpm)
                      Opacity
9:30
       9:45   10:00   10:15
                       Time
                  Parameters
           Steam Flow (klb/hr)
          Steam Temp (deg F)
              Coal Flow (Ib/hr)
              Boiler O2s (Avg)
                        west
                      central
                        east
 East Undergrate Air Flow (Ib/hr)
West Undergrate Air Flow (Ib/hr)
   Baghouse Inlet Temp (deg F)
 Baghouse Outlet Temp (deg F)
        Baghouse DP (in H2O)
   ID Fan Suet. Press, (in H2O)
   2A SDA Outlet Temp (deg F)
        2A Atomizer KW (KW)
              U2 % Solids (%)
           2A Lime Flow (gpm)
                      Opacity  9.74
277.3
956
29189
3.6
4.2
3
125148
128462
185.7
174
11
-26.2
185.5
66
35.2
5.5
9.53
Run #33







I

I
I
\



\

274.8
951
27692
3.8
4.7
2.8
126806
129713
184.4
173.5
12.9
-26.3
186.6
67
34.7
4.4


12:00
282.7
954
28421
2.7
2.8
2.5
121658
119808
183.9
173.3
11.6
-26.6
182.5
72
34.1
4.3
275.4
950
27000
4.1
4.7
3.4
125666
128341
NA
174.1
10.8
-26.1
186.5
66
33.1
2.4


12:15
278.3
950
30000
2.8
3
2.6
122456
120456
183.9
174.2
10.4
-15.3
187.1
71
36.6
2.3
270.5
948
27000
4.3
4.7
3.9
124467
127020
NA
173.5
11.4
-26.4
185.6
67
35.7
3.5


12:30
276.4
959
26341
2.7
3.2
2.2
124716
127160
185.5
171.7
10.9
-26.3
186.3
67
34.2
4.8
276.3
947
27692
4.2
4.4
4
124832
127069
185.6
172.2
11.4
-26.3
183
65
35
4.1


12:45
277.8
958
27692
2.8
3.3
2.2
122954
125325
183.1
171.8
9.9
-25.9
182.2
70
33.2
4.7
273.5
953
30000
4.0
4.5
3.4
126596
126943
184.2
174.2
11.5
-26.5
183
66
32.7
2.9


13:00
274.6
961
34839
2.5
2.9
2.1
123898
125193
187.4
174.5
11
-19.2
184.2
71
36.2
2.7


















13:15
274.4
950
28421
2.8
3.5
2
124570
127786
185.2
177.7
10.2
-25.4
186.2
66
34.9
6.8
                                            Run #32 Avg
                                                274.6
                                                950.8
                                               28095.5
                                                 4.0
                                                 4.5
                                                 3.4
                                               #DIV/0!
                                              125585.8
                                              127924.7
                                                185.0
                                                173.6
                                                 11.5
                                                -26.3
                                                185.0
                                                 66.0
                                                 34.4
                                                 3.8
                                                                                       Run #33 Avg
                                                277.4
                                                955.3
                                               29285.7
                                                 2.7
                                                 3.1
                                                 2.3
                                               #DIV/0!
                                               123375.3
                                               124288.0
                                                184.8
                                                173.9
                                                 10.7
                                                -23.1
                                                184.8
                                                 69.5
                                                 34.9
                                                 4.3
                                         RCA#2 APPENDIX A

-------
                       Time
                  Parameters
           Steam Flow (klb/hr)
          Steam Temp (deg F)
             Coal Flow (Ib/hr)
             Boiler O2s (Avg)
                        west
                      central
                        east
 East Undergrate Air Flow (Ib/hr)
West Undergrate Air Flow (Ib/hr)
   Baghouse Inlet Temp (deg F)
 Baghouse Outlet Temp (deg F)
        Baghouse DP (in H20)
   ID Fan Suet. Press, (in H2O)
   2A SDA Outlet Temp (deg F)
        2A Atomizer KW (KW)
             U2 % Solids (%)
          2A Lime Flow (gpm)
                     Opacity
                       Time
                  Parameters
           Steam Row (klb/hr)
          Steam Temp (deg F)
             Coal Flow (Ib/hr)
             Boiler O2s (Avg)
                        west
                      central
                        east
 East Undergrate Air Flow (Ib/hr)
West Undergrate Air Flow (Ib/hr)
   Baghouse Inlet Temp (deg F)
 Baghouse Outlet Temp (deg F)
        Baghouse DP (in H2O)
   ID Fan Suet. Press, (in H2O)
   2A SDA Outlet Temp (deg F)
        2A Atomizer KW (KW)
             U2 % Solids (%)
          2A Lime Row (gpm)
                     Opacity
Run #34
15:00
275.8
964
29189
2.8
: 3.1
2.5
123531
124870
184.5
175.5
10.9
-26.1
184.6
68
35.5
4.5
9.38
Run #35
9:00
276.8
948
28421
3.7
: 3.3
4.1

119739
122163
187.1
174.2
10.2
-25.1
185.1
62
35.4
5.6
8.52

15:15
275.5
956
30000
3.4
4.2
2.6
121363
120375
184.9
175.8
10.8
-26.1
185.4
69
36.1
6.1


9:15
275.6
954
30000
3.5
3.3
3.7

120992
121981
185
175.7
10.6
-25
184.6
64
33.4
5.5


15:30
276.9
952
29189
3.5
4.1
2.9
121472
119250
184.7
175.9
11.1
-26.1
184.2
70
35.3
4.7


9:30
276.7
947
27692
3.6
3.4
3.7

119364
120746
182.7
175.6
10.7
-24.9
184
65
33.5
4.6


15:45
275.9
950
27000
3.5
4.2
2.8
121199
118819
184.5
174.8
10.7
-25.9
181.2
70
35.7
6.9


9:45
276.7
953
29189
3.3
3.1
3.6
3.1
120487
120213
183.4
176.1
10.4
-25.7
184.8
65
34.6
5.6


16:00
276.4
952
27692
3.5
3.9
3
121308
119044
186.1
175.5
10.1
-25.4
186
69
35.1
6.2


10:00
274.3
951
28421
3.0
3.4
3.6
2
118951
119794
185.9
176.1
12
-26.1
185.8
63
35.3
6.1


16:15
277.8
952
27692
3.6
4.3
2.9
120323
119393
184.8
174.7
10.3
-26
186.8
67
34.5
4.7


10:15
272.1
955
29189
3.6
3.4
3.8

119813
118767
184
175.9
11.4
-25.8
186
64
36.2
5.9

                                                                                       Run #34 Avg
  276.4
  954.3
28460.3
   3.4
   4.0
   2.8
#DIV/0!
121532.7
120291.8
  184.9
  175.4
  10.7
  -25.9
  184.7
  68.8
  35.4
   5.5
                                                                                       Run #35 Avg
  275.4
  951.3
28818.7
   3.4
   3.3
   3.8
   2.6
119891.0
120610.7
  184.7
  175.6
  10.9
  -25.4
  185.1
  63.8
  34.7
   5.6
                                   RCA#2 APPENDIX A

-------
                            Run #36
                       Time 11:15
                  Parameters
           Steam Flow (klb/hr)
          Steam Temp (deg F)
              Coal Flow (Ib/hr)
              Boiler O2s (Avg)
                        west
                      central
                        east
 East Undergrate Air Flow (Ib/hr) 119001
West Undergrate Air Flow (Ib/hr)
   Baghouse Inlet Temp (deg F)
 Baghouse Outlet Temp (deg F)
        Baghouse DP (in H2O)
   ID Fan Suet. Press, (in H2O)
   2A SDA Outlet Temp (deg F)
        2A Atomizer KW (KW)
              U2 % Solids (%)
          2A Lime Row (gpm)
                      Opacity
                       Time
                  Parameters
           Steam Row (klb/hr)
          Steam Temp (deg F)
              Coal Flow (Ib/hr)
              Boiler O2s (Avg)
                        west
                      central
                        east
 East Undergrate Air Flow (Ib/hr)
West Undergrate Air Flow (Ib/hr)
   Baghouse Inlet Temp (deg F)
  Baghouse Outlet Temp (deg F)
        Baghouse DP (in H2O)
    ID Fan Suet. Press, (in H2O)
   2A SDA Outlet Temp (deg F)
        2A Atomizer KW (KW)
              U2 % Solids (%)
           2A Lime Flow (gpm)
                      Opacity
11:30  11:45   12:00  12:15
274.3
957
29189
3.3
2.8
3.7
119001
122334
186.6
175.4
11.8
-26.4
185.4
64
33.5
6.1
10.49
ton #37
23:30
202.3
952
19286
5.4
5.6
5.2

99793
98370
184.4
172.6
5.9
-16.5
185.3
50
33.2
6.6
9.65
273.7
943
26341
3.4
3.1
3.6
119355
120291
182.5
176.6
15.2
-26
183.9
64
33.4
4.8


23:45
203.4
948
19286
5.3
5.2
5.3

100394
99762
184.5
173.7
7.7
•16.3
180.4
57
35.8
5.6

269.1
952
28421
3.7
3.4
4
118559
120378
186.4
176.5
11.4
-25.7
184.5
68
32.7
5.1


0:15
208.5
952
19636
4.5
5.2
5.2
3.2
101188
99446
185.9
173.7
6.3
-17.2
185.2
50
33.5
3.2

270.6
952
29189
3.9
3.3
4.4
120340
118642
183.7
174.9
10.7
-25
184.5
69
36.5
6


0:30
206.6
952
20000
4.8
5
5.5
3.8
102053
100128
184
173
6.1
-17
184
47
34.8
6.6

275.8
951
27000
3.4
2.7
4.1
120414
121709
185.5
173.3
11.2
-25.6
182.6
70
35.3
5.6


0:45
204
952
20000
4.9
5.2
5.4
4
100947
98108
186.9
173.1
5.3
-16
187
44
36.9
5.9

                                                   Run #36 Avg
                                                      272.7
                                                      951.0
                                                     28028.0
                                                       3.5
                                                       3.1
                                                       4.0
                                                     #DIV/0!
                                                     119533.8
                                                     120670.8
                                                      184.9
                                                      175.3
                                                       12.1
                                                      -25.7
                                                      184.2
                                                       67.0
                                                       34.3
                                                       5.5
                                                                                       Run #37 Avg
                                                       205.0
                                                       951.2
                                                     19641.6
                                                        5.0
                                                        5.2
                                                        5.3
                                                        3.7
                                                     100875.0
                                                     99162.8
                                                       185.1
                                                       173.2
                                                        6.3
                                                       -16.6
                                                       184.4
                                                       49.6
                                                       34.8
                                                        5.6
                                         RCA#2 APPENDIX A

-------
                            Run #38
                       Time  1:45
                  Parameters
           Steam Flow (klb/hr)
          Steam Temp (deg F)
             Coal Flow (Ib/hr)
             Boiler 02s (Avg)
                        west
                      central
                        east
 East Undergrate Air Flow (Ib/hr)
West Undergrate Air Flow (Ib/hr)
   Baghouse Inlet Temp (deg F)
 Baghouse Outlet Temp (deg F)
        Baghouse DP (in H2O)
   ID Fan Suet. Press, (in H2O)
   2A SDA Outlet Temp (deg F)
        2A Atomizer KW (KW)
             U2 % Solids (%)
          2A Lime Flow (gpm)
                     Opacity
                       Time
                  Parameters
           Steam Flow (klb/hr)
          Steam Temp (deg F)
              Coal Flow (Ib/hr)
              Boiler O2s (Avg)
                        west
                      central
                        east
 East Undergrate Air Flow (Ib/hr)
West Undergrate Air Flow (Ib/hr)
   Baghouse Inlet Temp (deg F)
 Baghouse Outlet Temp (deg F)
        Baghouse DP (in H2O)
   ID Fan Suet. Press, (in H2O)
   2A SDA Outlet Temp (deg F)
        2A Atomizer KW (KW)
              U2 % Solids (%)
           2A Lime Flow (gpm)
                     Opacity
2:00
      2:15
2:30    2:45
                          3:00
207.3
947
20000
4.8
5
5.4
4.1
101488
98470
185.7
173.4
5.2
-15.9
182.2
52
33.2
4.6
7.84
lun #39
3:45
203.3
951
19636
5.1
5.1
5.3
5
101257
100145
186.7
173
5.6
-16.1
186.1
51
34.3
7.1
7.76
200.6
951
19286
4.8
4.9
5.2
4.2
100871
98661
186.1
173.5
5.6
-16.2
188.1
49
35.4
5.4


4:00
202.4
949
20377
5.1
4.7
5.1
5.5
101339
100764
184.3
173.9
5.7
-16.4
185.6
50
35.4
5.3

202.4
949
19636
5.0
5.2
5.3
4.4
100400
98714
184.8
174.5
5.9
-16.5
190.8
48
35.6
5.5


4:15
206.4
952
20769
4.9
4
5.2
5.6
101440
101029
183.4
173.4
5.2
-15.8
186
49
36.1
5.4

203.8
954
19636
5.0
5
5.5
4.4
100204
97735
184.7
173.4
5.4
-16
185.2
49
35.9
5.3


4:30
208.3
952
20377
4.9
3.7
5
5.9
101983
100248
183.1
173.4
6.1
-16.7
184.2
50
33.6
3.1

203.2
951
20000
5.0
5.2
5.4
4.3
101418
98900
185.8
173.4
5.9
-10.5
184
50
33.1
4.4


4:45
205.9
951
19636
5.0
4.2
5.1
5.7
102443
99858
183.4
173.3
5.1
-15.9
189.5
48
33.4
5.1

208.5
949
19286
4.9
4.9
5.3
4.6
100175
98167
185.9
174.5
5.2
-15.8
183.1
51
35.7
3.7


5:00
209.3
951
20769
4.9
4.3
5
5.3
101803
99948
186.6
172.8
6.2
-17.3
187.4
47
34.1
4.9

                                                   Run #38 Avg
                                                      204.3
                                                      950.2
                                                     19640.7
                                                       4.9
                                                       5.0
                                                       5.4
                                                       4.3
                                                     100759.3
                                                     98441.2
                                                      185.5
                                                      173.8
                                                       5.5
                                                      -15.2
                                                      185.6
                                                      49.8
                                                      34.8
                                                       4.8
                                                                                       Run #39 Avg
                                                      205.9
                                                      951.0
                                                     20260.7
                                                       5.0
                                                       4.3
                                                       5.1
                                                       5.5
                                                     101710.8
                                                     100332.0
                                                      184.6
                                                      173.3
                                                       5.7
                                                      -16.4
                                                      186.5
                                                       49.2
                                                       34.5
                                                       5.2
                                    RCA#2 APPENDIX A

-------
                       Time
                  Parameters
           Steam Flow (klb/hr)
          Steam Temp (deg F)
             Coal Flow (Ib/hr)
             Boiler 02s (Avg)
                        west
                     central
                        east
 East Undergrate Air Flow (Ib/hr)
West Undergrate Air Flow (Ib/hr)
   Baghouse Inlet Temp (deg F)
 Baghouse Outlet Temp (deg F)
        Baghouse DP (in H2O)
   ID Fan Suet. Press, (in H2O)
   2A SDA Outlet Temp (deg F)
        2A Atomizer KW (KW)
             U2 % Solids (%)
          2A Lime Flow (gpm)
                     Opacity
                       Time
                  Parameters
           Steam Flow (klb/hr)
          Steam Temp (deg F)
              Coal Row (Ib/hr)
              Boiler O2s (Avg)
                        west
                      central
                        east
 East Undergrate Air Flow (Ib/hr)
West Undergrate Air Flow (Ib/hr)
   Baghouse Inlet Temp (deg F)
 Baghouse Outlet Temp (deg F)
        Baghouse DP (in H2O)
   ID Fan Suet. Press, (in H2O)
   2A SDA Outlet Temp (deg F)
        2A Atomizer KW (KW)
              U2 % Solids (%)
          2A Lime Flow (gpm)
                      Opacity
Run #40
9:00
218.2
959
24000
4.5
: 4
7.8
1.8
103534
99769
185.1
176
5.4
-16.2
186.7
50
35.4
1.1
Run #41
11:15
1
199.8
950
20000
5.0
: 6.3
6
: 2.7
i 98426
96231
I 187.7
I 176.6
I 7.3
-16.9
190.6
52
I 35.7
1.9

9:15
177.9
964
18305
5.6
6.4
5.2
5.3
97013
94466
186.5
174.9
4.9
-14.7
' 185.7
46
34.8
9.7

11:30
204.9
949
19636
4.9
6.4
5.7
2.5
98034
97526

176.4
5.4
-16.4
182.6
53
34.9
6.8

9:30
128.4
942
12857
8.2
8.8
7.3
8.5
86327
83607
183.8
175.6
4.4
-12.7
183.9
43
35.4
9.7

11:45
208.4
947
19636
4.8
6.5
5.5
2.4
99368
96381
183
176.3
6
-17.2
183.9
54
34.3
3.7

9:45
205
944
20769
5.6
5.1
8.3
3.4
101109
96746
184.8
176
5.2
-15
187.1
45
35
9.7

12:00
211.6
947
19286
4.5
6.4
5.3
1.9
100741
98661
175
175.3
5,5
-16.3
179.7
59
35.5
0.9

10:00
214.5
950
20769
4.2
4.3
5.6
2.7
102241
100094
183.2
175.5
6
-16.8
188.4
47
34.6
9.7

12:15
239
967
28421
4.8
3.9
5.6

107541
107168
184.2
175.6
7.1
-18.5
186.2
58
35.6
7.9

10:15
252.3
956
33750
4.6

4.6

119823
120164
185
178.2
8.7
-20.8
184.8
56
34.6
0.6

12:30
243.8
935
24545
4.0
4.3
3.7

106003
105497
183
174.9
9.4
-21.1
185.7
56
35.7
6.1
                                                                                       Run #40 Avg
  199.4
  952.5
21741.7
   5.5
   5.7
   6.5
   4.3
101674.5
99141.0
  184.7
  176.0
   5.8
  -16.0
  186.1
  47.8
  35.0
   6.8
                                                                                       Run #41 Avg
  217.9
  949.2
 21920.7
   4.7
   5.6
   5.3
   2.4
101685.5
100244.0
  182.6
  175.9
   6.8
  -17.7
  184.8
  55.3
  35.3
   4.6
                                         RCA#2 APPENDIX A

-------
                       Time
                  Parameters
           Steam Flow (klb/hr)
          Steam Temp (deg F)
              Coal Row (Ib/hr)
              Boiler O2s (Avg)
                        west
                      central
                        east
 East Undergrate Air Flow (Ib/hr)
West Undergrate Air Flow (Ib/hr)
   Baghouse Inlet Temp (deg F)
 Baghouse Outlet Temp (deg F)
        Baghouse DP (in H20)
   ID Fan Suet. Press, (in H2O)
   2A SDA Outlet Temp (deg F)
        2A Atomizer KW (KW)
              U2 % Solids (%)
          2A Lime Flow (gpm)
                     Opacity
Run #42
14:00
243.5
956
28421
4.1
4
4.2
111401
1 12460
182.8
179
9
-20.1
183.6
57
36.5
6.9
14:15
208.2
928
18947
4.3
6.2
2.3
104184
103783
185.1
177.2
9.3
-12.2
183.8
56
35.7
3.9
14:30
212.7
942
20000
4.9
5.8
3.9
99591
98088
184.5
177.4
6.8
-17.2
184.5
55
33.6
0.9
14:45
216.1
950
21176
4.9
5.6
4.1
100395
99436
185.2
177.8
72,
-18.1
190.9
52
35
8.6
15:00
204.7
955
21600
4.9
5.2
4.5
99218
98256
185.2
177.2
6.6
-16.3
193.5
53
35.1
5.7
                                                                                      Run #42 Avg
  217.0
  946.2
22028.8
   4.6
   5.4
   3.8
#DIV/0!
102957.8
102404.6
  184.6
  177.7
   7.8
  -16.8
  187.3
  54.6
  35.2
   5.2
                                  RCA#2 APPENDIX A

-------
                                RCA #2 Appendix B
                   Computer Results for M17 Tests
MRJ-OPPT\R4703-02-07 Appendices Covers WPD

-------
FILE NAME - 30A
RUN # - 30 - Method 17 Train A for PM
LOCATION - Unit 2A Baghouse Outlet Duct
DATE - 11/16/99 Time: 1215-1405
PROJECT # - 104703.1.002.05.01

Initial Meter Volume  (Cubic Feet)=         203.524
Final Meter Volume  (Cubic Feet)=           238.517
Meter Factor=                                 0.996
Final Leak Rate (cu ft/min)=                  0.004
Net Meter Volume  (Cubic Feet)=              34.853
Gas Volume (Dry Standard Cubic Feet)=       35.365

Barometric Pressure  (in Hg)=                  29.65
Static Pressure (Inches H20) =               -25.90

Percent Oxygen=                                4 . 2
Percent Carbon Dioxide=                       15.1
Moisture Collected  (ml)=                      93.7
Percent Water=                                11.1

Average Meter Temperature  (F)=                   56
Average Delta H (in H20)=                     0.49
Average Delta P (in H20)=                     1.567
Average Stack Temperature  (F)=                 178

Dry Molecular Weight=                         30.58
Wet Molecular Weight=                         29.19

Average Square Root of Delta P  (in H20)=    1.1623
% Isokinetic=                                 100.3

Pitot Coefficient=                            0.84
Sampling Time  (Minutes)=                      100.0
Nozzle Diameter (Inches)=                     0.146
Stack Axis #1  (Inches)=                       57.0
Stack Axis #2  (Inches)=                       66.0
Rectangular Stack
Stack Area (Square Feet)=                     26.13

Stack Velocity  (Actual, Feet/min)=           4,444
Flow Rate  (Actual, Cubic ft/min)=          116,110
Flow rate  (Standard, Wet, Cubic ft/min)=    89,113
Flow Rate  (Standard, Dry, Cubic ft/min)=    79,227

Particulate Loading - Front Half

Particulate Weight  (g)=                     0.0409
Particulate Loading, Dry Std.  (gr/scf)=     0.0178
Particulate Loading, Actual  (gr/cu ft)=     0.0121
Emission Rate  (lb/hr)=                        12.09

No Back Half Analysis
PROG.=VER 06/27/89
11-23-1999  08:57:18
Corr. to 7% 02 & 12% C02
     0.0148    0.0142
                            RCA#2 APPENDIX B

-------
                         * * METRIC UNITS * *
 FILE NAME  -  30A
 RUN #  -  30  - Method 17 Train A for PM
 LOCATION -  Unit 2A Baghouse Outlet Duct
 DATE - 11/16/99 Time:  1215-1405
 PROJECT  #  -  104703.1.002.05.01

 Initial  Meter Volume (Cubic Meters)=
 Final Meter  Volume (Cubic Meters)=
 Meter Factor=
 Final Leak Rate (cu m/min)=
 Net Meter Volume (Cubic Meters)=
 Gas Volume  (Dry Standard Cubic Meters)=

 Barometric Pressure (mm Hg)=
 Static Pressure (mm H20)=

 Percent  Oxygen=
 Percent  Carbon Dioxide=
 Moisture Collected (ml)=
 Percent  Water=

 Average  Meter Temperature (C)=
 Average  Delta H (mm H20) =
 Average  Delta P (mm H20)=
 Average  Stack Temperature (C) =

 Dry Molecular Weight=
 Wet Molecular Weight=

 Average  Square Root of  Delta P (mm H20)=
 % Isokinetic=

 Pitot Coefficient=
 Sampling Time (Minutes)=
 Nozzle Diameter (mm)=
 Stack Axis #1 (Meters)=
 Stack Axis #2 (Meters)=
 Rectangular  Stack
 Stack Area  (Square  Meters)=

 Stack Velocity  (Actual,  m/min)=
'Flow rate  (Actual,  Cubic m/min) =
 Flow rate  (Standard, Wet,  Cubic  m/min)=
 Flow rate  (Standard, Dry,  Cubic  m/min)=

 Particulate  Loading -  Front  Half

 Particulate  Weight  (g)=
 Particulate  Loading, Dry Std.  (mg/cu m)=
 Particulate  Loading, Actual  (mg/cu m)=
 Emission Rate (kg/hr)=

 No Back Half  Analysis
          PROG.=VER  06/27/89
          11-23-1999   08:57:18
 5.763
 6.754
 0.996
0.0001
 0.987
 1.001

   753
  -658

   4.2
  15.1
  93.7
  11.1

    13
  12.5
  39.8
    81

 30.58
 29.19

5.8578
 100.3

  0.84
 100.0
  3.71
 1.448
 1.676

 2.427

 1,355
 3,288
 2,523
 2,243
0.0409
  40.8
  27.9
  5.49
Corr. to 7% 02 & 12% C02
       34.0      32.5
                                RCA#2 APPENDIX B

-------
FILE NAME - 30A
RUN # - 30 - Method 17 Train A  for PM
LOCATION - Unit 2A Baghouse Outlet Duct
DATE - 11/16/99 Time: 1215-1405
PROJECT # - 104703.1.002.05.01
Point #

 1
 2
 3
 4
 5
 6
 7
 8
 9
 10
 11
 12
 13
 14
 15
 16
 17
 18
 19
 20
 21
 22
 23
 24
 25
                                  PROG.=VER 06/27/89
                                  11-23-1999  08:57:18
Delta P
in. H20)
2.300
2.200
1.700
0.650
0.050
2.500
2.400
2.100
0.770
0.100
2.500
2.500
2.400
1.500
0.230
2.400
2.300
2.200
1.200
0.170
2.300
2.100
1.800
0.680
0. 120
Delta H
(in. H20)
0.72
0.69
0.53
0.20
0.01
0 .78
0.75
0.66
0.24
0.03
0.79
0.79
0.76
0.47
0.07
0.76
0.72
0.69
0.38
0.05
0.73
0.67
0.57
0.21
0.03
Stack
(F)
174
177
177
177
175
178
178
178
176
175
178
179
179
180
180
180
180
180
179
178
180
178
177
178
178
T
In(F)
51
52
53
53
54
53
54
55
57
57
55
57
58
59
59
58
58
60
60
60
59
61
61
62
61
Meter T
Out (F)
51
52
53
52
53
53
53
54
54
54
54
55
55
55
56
56
56
57
57
57
58
58
58
58
58
Fraction

DRY CATCH
FILTER

Fraction

PROBE RINSE
IMPINGERS
 Final Wt.  Tare Wt.  Blank Wt. Net Wt,
  (g)         (g)        (g)       (g)
0.0000    0.0000    0.0000    0.0000
3.3508    3.3137    0.0000    0.0371
 Final Wt
  (g)
3 .6645
0.0000
   Tare Wt.
Probe Rinse Blank  (mg/ml)=
Impinger Blank  (mg/ml)=   0.0000
    (g)
  3.6607
  0.0000
0.0000
  Vol.
 (ml)
31.6
 0.0
  Net Wt
   (g)
0.0038
0.0000
                             RCA#2 APPENDIX B

-------
FILE NAME - SOB
RUN # - 30 - Method 17 Train B for PM
LOCATION - Unit 2A Baghouse Outlet Duct
DATE - 11/16/99 Time: 1217-1407
PROJECT # - 104703.1.002.05.02

Initial Meter Volume  (Cubic Feet)=          823.925
Final Meter Volume  (Cubic Feet)=            859.009
Meter Factor=                                 1.010
Final Leak Rate (cu ft/min)=                  0.005
Net Meter Volume  (Cubic Feet)=               35.435
Gas Volume (Dry Standard Cubic Feet)=        35.886

Barometric Pressure  (in Hg)=                  29.65
Static Pressure (Inches H20)=                -25.90

Percent Oxygen=                                4 . 2
Percent Carbon Dioxide=                        15.1
Moisture Collected  (ml)=                       94.5
Percent Water=                                 11.0

Average Meter Temperature  (F)=                   57
Average Delta H (in H20)=                      0.51
Average Delta P (in H20)=                     1.584
Average Stack Temperature  (F)=                 180

Dry Molecular Weight=                         30.58
Wet Molecular Weight=                         29.20

Average Square Root of Delta P  (in H20)=     1.1713
% Isokinetic=                                 101.1

Pitot Coefficient=                             0.84
Sampling Time  (Minutes)=                      100.0
Nozzle Diameter (Inches)=                     0.146
Stack Axis #1  (Inches)=                        57.0
Stack Axis #2  (Inches)=                        66.0
Rectangular Stack
Stack Area (Square Feet)=                     26.13

Stack Velocity  (Actual, Feet/min)=           4,486
Flow Rate (Actual, Cubic ft/min)=           117,207
•Flow rate (Standard, Wet, Cubic ft/min)=     89,629
Flow Rate (Standard, Dry, Cubic ft/min)=     79,739

Particulate Loading - Front Half

Particulate Weight  (g)=                      0.0335
Particulate Loading, Dry Std.  (gr/scf)=      0.0144
Particulate Loading, Actual  (gr/cu ft)=      0.0098
Emission Rate  (lb/hr)=                         9.82

No Back Half Analysis
PROG.=VER 06/27/89
11-23-1999  08:57:32
Corr. to 7% 02 & 12% C02
     0.0120    0.0114
                                RCA#2 APPENDIX B

-------
                        * * METRIC UNITS * *
FILE NAME - 3 OB
RUN # - 30 - Method 17 Train B for PM
LOCATION - Unit 2A Baghouse Outlet Duct
DATE - 11/16/99 Time: 1217-1407
PROJECT # - 104703.1.002.05.02

Initial Meter Volume  (Cubic Meters)=
Final Meter Volume  (Cubic Meters)=
Meter Factor=
Final Leak Rate (cu m/min)=
Net Meter Volume  (Cubic Meters)=
Gas Volume  (Dry Standard Cubic Meters)=

Barometric Pressure  (mm Hg)=
Static Pressure (mm H20)=

Percent Oxygen=
Percent Carbon Dioxide=
Moisture Collected  (ml)=
Percent Water=
          PROG.=VER 06/27/89
          11-23-1999  08:57:32
Average Meter Temperature  (C)=
Average Delta H  (mm H20)=
Average Delta P  (mm H20)=
Average Stack Temperature  (C)=

Dry Molecular Weight=
Wet Molecular Weight=

Average Square Root of Delta  P  (mm  H20);
% Isokinetic=

Pitot Coefficient=
Sampling Time  (Minutes)=
Nozzle Diameter  (mm)=
Stack Axis #1  (Meters)=
Stack Axis #2  (Meters)=
Rectangular Stack
Stack Area  (Square Meters)=

Stack Velocity   (Actual, m/min)=
Flow rate  (Actual, Cubic m/min)=
Flow rate  (Standard, Wet,  Cubic m/min)=
Flow rate  (Standard, Dry,  Cubic m/min)=

Particulate Loading - Front Half

Particulate Weight  (g)=
Particulate Loading, Dry Std.  (mg/cu m)
Particulate Loading, Actual  (mg/cu  m)=
Emission Rate  (kg/hr)=

No Back Half Analysis
23.330
24.324
 1.010
0.0001
 1.003
 1.016

   753
  -658

   4.2
  15.1
  94.5
  11.0

    14
  13.0
  40.2
    82

 30.58
 29.20

5.9032
 101.1

  0.84
 100.0
  3.71
 1.448
 1.676

 2.427

 1,367
 3,319
 2,538
 2,258
0.0335
  33.0
  22.4
  4.46
Corr. to 7% 02
       27.5
& 12% C02
  26.2
                            RCA#2 APPENDIX B

-------
 FILE  NAME  -  3 OB
 RUN # -  30  -  Method 17 Train B for PM
 LOCATION -  Unit 2A Baghouse Outlet Duct
 DATE  - 11/16/99 Time:  1217-1407
 PROJECT  #  -  104703.1.002.05.02
 Point  #

  1
  2
  3
  4
  5
  6
  7
  8
  9
  10
  11
  12
  13
  14
  15
  16
  17
  18
  19
  20
  21
  22
  23
  24
  25
                                   PROG.=VER 06/27/89
                                   11-23-1999  08:57:32
Delta P
(in. H20)
2.600
2.500
2.100
1.100
0.160
2.400
2.000
1.800
0.730
0.120
2.300
2.100
1.800
0.680
0.100
2.300
2.200
2.100
0.930
0.130
2.700
2.600
2.300
1.700
0.150
Delta H
(in. H20)
0.85
0.81
0.68
0.35
0.05
0.78
0.65
0.58
0.23
0.03
0.75
0.68
0.58
0.22
0.03
0.75
0.71
0.68
0.30
0 . 04
0.88
0.85
0.75
0.55
0.04
Stack
(F)
177
179
180
179
178
178
181
179
178
178
179
182
182
182
182
182
182
182
181
180
182
180
181
182
181
T Meter T
In(F)
54
54
55
55
55
55
55
56
57
57
57
58
57
58
58
58
58
59
59
60
59
59
61
62
62
Out (F)
53
54
54
55
55
55
55
55
56
56
56
57
56
57
57
57
57
58
58
58
59
59
60
60
60
Fraction

DRY CATCH
FILTER

•Fraction

PROBE RINSE
IMPINGERS
 Final Wt.  Tare Wt.  Blank Wt. Net Wt,
  (g)        (g)        (g)       (g)
0.0000    0.0000    0.0000    0.0000
3.3408    3.3087    0.0000    0.0321
 Final Wt.  Tare Wt.
  (g)
3.5871
0.0000
Probe Rinse Blank  (mg/ml)=
Impinger Blank  (mg/ml)=   0.0000
    (g)
  3.5857
  0.0000
0.0000
  Vol.
 (ml)
31.5
 0.0
  Net Wt
   (g)
0.0014
0.0000
                                RCA#2 APPENDIX B

-------
FILE NAME - 31A
RUN # - 31 - Method 17 Train A for PM
LOCATION - Unit 2A Baghouse Outlet Duct
DATE - 11/16/99 Time: 1520-1645
PROJECT # - 104703.1.002.05.01

Initial Meter Volume  (Cubic Feet)=         238.859
Final Meter Volume  (Cubic Feet)=           266.079
Meter Factor=                                0.996
Final Leak Rate (cu ft/min)=                 0.002
Net Meter Volume  (Cubic Feet)=              27.111
Gas Volume (Dry Standard Cubic Feet)=       27.394

Barometric Pressure  (in Hg)=                 29.60
Static Pressure (Inches H20)=               -26.00

Percent Oxygen=                                4 . 5
Percent Carbon Dioxide=                       14.6
Moisture Collected  (ml)=                      81.1
Percent Water=                                12 . 2

Average Meter Temperature  (F)=                   57
Average Delta H (in H20)=                     0.52
Average Delta P (in H20)=                    1.640
Average Stack Temperature  (F) =                 177

Dry Molecular Weight=                        30.52
Wet Molecular Weight=                        28.98

Average Square Root of Delta P  (in H20)=    1.1986
% Isokinetic=                                101.5

Pitot Coefficient=                            0.84
Sampling Time (Minutes)=                      75.0
Nozzle Diameter (Inches)=                    0.146
Stack Axis #1 (Inches)=                       57.0
Stack Axis #2 (Inches)=                       66.0
Rectangular Stack
Stack Area (Square Feet)=                    26.13

Stack Velocity  (Actual, Feet/min)=          4,601
Flow Rate (Actual, Cubic ft/min)=          120,207
Flow rate (Standard, Wet, Cubic ft/min)=    92,182
Flow Rate (Standard, Dry, Cubic ft/min)=    80,901

Particulate Loading - Front Half

Particulate Weight  (g)=                     0.0293
Particulate Loading, Dry Std.  (gr/scf)=     0.0165
Particulate Loading, Actual  (gr/cu ft) =     0.0111
Emission Rate (lb/hr)=                       11.42

No Back Half Analysis
PROG.=VER 06/27/89
11-23-1999  08:57:46
Corr. to 7% 02 & 12% C02
     0.0140    0.0135
                            RCA#2 APPENDIX B

-------
                         *  *  METRIC UNITS  *  *
FILE NAME  -  31A
RUN #  - 31 - Method  17  Train A for PM
LOCATION - Unit 2A Baghouse  Outlet Duct
DATE - 11/16/99 Time: 1520-1645
PROJECT #  -  104703.1.002.05.01

Initial Meter Volume  (Cubic  Meters)=          6.764
Final Meter Volume  (Cubic  Meters)=           7.534
Meter Factor=                                 0.996
Final Leak Rate (cu m/min)=                 0.0001
Net Meter Volume  (Cubic  Meters)=              0.768
Gas Volume (Dry Standard Cubic Meters)=       0.776

Barometric Pressure  (mm  Hg)=                   752
Static Pressure (mm H20) =                      -660

Percent Oxygen=                                4.5
Percent Carbon  Dioxide=                        14.6
Moisture Collected  (ml)=                      81.1
Percent Water=                                 12.2

Average Meter Temperature  (C)=                  14
Average Delta H (mm H20)=                      13.1
Average Delta P (mm H20)=                      41.6
Average Stack Temperature  (C) =                  81

Dry Molecular Weight=                         30.52
Wet Molecular Weight=                         28.98

Average Square  Root of Delta P (mm H20) =    6.0409
% Isokinetic=                                 101.5

Pitot Coefficient=                             0.84
Sampling Time  (Minutes)=                      75.0
Nozzle Diameter (mm)=                          3.71
Stack Axis #1  (Meters)=                       1.448
Stack Axis #2  (Meters)=                       1.676
Rectangular Stack
Stack Area (Square Meters)=                   2.427

Stack Velocity   (Actual, m/min)=              1,402
•Flow rate  (Actual, Cubic m/min) =              3,404
Flow rate  (Standard, Wet,  Cubic m/min)=       2,610
Flow rate  (Standard, Dry,  Cubic m/min)=       2,291

Particulate Loading - Front  Half

Particulate Weight  (g)=                     0.0293
Particulate Loading, Dry Std.  (mg/cu  m)=       37.8
Particulate Loading, Actual  (mg/cu m)=        25.4
Emission Rate  (kg/hr)=                         5.18

No Back Half Analysis
PROG.=VER 06/27/89
11-23-1999  08:57:46
Corr. to 7% 02 & 12% C02
       32.1      31.0
                                RCA#2 APPENDIX B

-------
FILE NAME - 31A
RUN # - 31 - Method 17 Train A  for  PM
LOCATION - Unit 2A Baghouse Outlet  Duct
DATE - 11/16/99 Time: 1520-1645
PROJECT # - 104703.1.002.05.01
                                  PROG.=VER 06/27/89
                                  11-23-1999   08:57:46
'oint #

1
2
3
4
5
6
7
8
9
10
11
12
13
14
15
16
17
18
19
20
21
22
23
24
25
Delta P
(in
2.
2.
2.
1.
0.
2.
2.
2.
0.
0.
2.
1.
2.
0.
0.
2.
2.
2.
1.
0.
2.
2.
2.
1.
0.
. H20)
500
400
100
700
220
500
100
100
840
090
300
900
000
650
040
400
100
200
000
190
500
600
400
800
360
Delta H
(in.
0.
0.
0.
0.
0.
0.
0.
0.
0.
0.
0.
0.
0.
0.
0.
0.
0.
0.
0.
0.
0.
0.
0.
0.
0.
H20)
79
75
66
54
06
79
66
66
26
02
73
60
63
20
01
76
66
70
31
06
79
82
76
57
11
Stack
(F)
178
179
178
177
177
178
178
177
177
178
178
177
178
176
177
177
177
178
179
178
177
177
177
177
169
T Meter T
In(F)
55
56
57
58
57
57
58
58
58
58
57
58
59
60
60
58
58
59
59
59
58
58
59
61
61
Out (F)
55
55
55
56
56
56
56
56
56
57
56
57
57
57
57
57
57
57
57
57
57
57
58
58
58
Fraction

DRY CATCH
FILTER

Fraction

PROBE RINSE
IMPINGERS
 Final Wt.  Tare Wt.  Blank Wt. Net Wt
  (g)         (g)        (g)       (g)
0.0000    0.0000    0.0000    0.0000
3.4017    3.3752    0.0000    0.0265
 Final Wt.
  (g)
3.6595
0.0000
        0
Probe Rinse Blank  (mg/ml)=
Impinger Blank  (trig/ml) =   0.0000
 Tare Wt,
  (g)
3.6567
0.0000
0000
  Vol.
 (ml)
22.2
 0.0
  Net Wt,
   (g)
0.0028
0.0000
                            RCA#2 APPENDIX B

-------
 FILE NAME  -  3 IB
 RUN #  -  31  -  Method 17  Train B for PM
 LOCATION - Unit 2A Baghouse Outlet Duct
 DATE - 11/16/99 Time: 1521-1646
 PROJECT  #  -  104703.1.002.05.02

 Initial  Meter  Volume (Cubic Feet)=         859.315
 Final Meter Volume (Cubic  Feet)=            886.812
 Meter Factor=                                 1.010
 Final Leak Rate (cu ft/min)=                 0.004
 Net Meter Volume (Cubic Feet)=              27.772
 Gas Volume  (Dry Standard Cubic Feet)=       28.037

 Barometric Pressure (in Hg)=                 29.60
 Static Pressure (Inches H20)=               -26.00

 Percent  Oxygen=                                4.5
 Percent  Carbon Dioxide=                       14.6
 Moisture Collected (ml)=                      73.7
 Percent  Water=                                11.0

 Average  Meter  Temperature  (F)=                  58
 Average  Delta  H (in H20)=                      0.49
 Average  Delta  P(inH20)=                     1.500
 Average  Stack  Temperature  (F)=                 180

 Dry Molecular  Weight=                         30.52
 Wet Molecular  Weight=                         29.14

 Average  Square Root of  Delta P (in H20) =     1.2232
 % Isokinetic=                                 100.8

 Pitot Coefficient=                            0.84
 Sampling Time  (Minutes)=                      75.0
 Nozzle Diameter (Inches)=                     0.146
 Stack Axis #1  (Inches)=                       57.0
 Stack Axis #2  (Inches)=                       66.0
 Rectangular Stack
 Stack Area  (Square Feet)=                     26.13

 Stack Velocity  (Actual, Feet/min)=          4,693
 Flow Rate  (Actual,  Cubic ft/min)=           122,606
Flow rate  (Standard, Wet,  Cubic ft/min)=     93,634
 Flow Rate  (Standard, Dry,  Cubic ft/min)=     83,318

 Particulate Loading - Front  Half

 Particulate Weight (g)=                     0.0188
 Particulate Loading, Dry Std.  (gr/scf)=     0.0103
 Particulate Loading, Actual  (gr/cu ft)=     0.0070
 Emission Rate  (lb/hr)=                         7.37

 No Back Half Analysis
                                                      PROG.=VER 06/27/89
                                                      11-23-1999  08:58:00
                                                     Corr. to 7% 02  & 12%  C02
                                                          0.0088     0.0085
10
                               RCA#2 APPENDIX B

-------
                        * * METRIC UNITS * *
FILE NAME - 3 IB
RUN # - 31 - Method 17 Train B for PM
LOCATION - Unit 2A Baghouse Outlet Duct
DATE - 11/16/99 Time: 1521-1646
PROJECT # - 104703.1.002.05.02

Initial Meter Volume  (Cubic Meters)=
Final Meter Volume  (Cubic Meters)=
Meter Factor=
Final Leak Rate (cu m/min)=
Net Meter Volume  (Cubic Meters)=
Gas Volume (Dry Standard Cubic Meters)=

Barometric Pressure  (mm Hg)=
Static Pressure (mm H20)=

Percent Oxygen=
Percent Carbon Dioxide=
Moisture Collected  (ml)=
Percent Water=
          PROG.=VER 06/27/89
          11-23-1999  08:58:00
Average Meter Temperature  (C)=
Average Delta H  (mm H20)=
Average Delta P  (mm H20)=
Average Stack Temperature  (C) =

Dry Molecular Weight=
Wet Molecular Weight=

Average Square Root of Delta P  (mm H20)=
% Isokinetic=

Pitot Coefficient=
Sampling Time  (Minutes)=
Nozzle Diameter  (mm)=
Stack Axis #1  (Meters)=
Stack Axis #2  (Meters)=
Rectangular Stack
Stack Area  (Square Meters)=

Stack Velocity   (Actual, m/min)=
Flow rate  (Actual, Cubic m/min)=
Flow rate  (Standard, Wet,  Cubic m/min)=
Flow rate  (Standard, Dry,  Cubic m/min)=

Particulate Loading - Front Half

Particulate Weight  (g)=
Particulate Loading, Dry Std.  (mg/cu m)=
Particulate Loading, Actual  (mg/cu m)=
Emission Rate  (kg/hr)=

No Back Half Analysis
24.332
25.111
 1.010
0.0001
 0.786
 0.794

   752
  -660

   4.5
  14.6
  73 .7
  11.0

    14
  12.4
  38.1
    82

 30.52
 29.14

6.1649
 100.8

  0.84
  75.0
  3 .71
 1.448
 1.676

 2.427

 1,430
 3,472
 2,651
 2,359
0.0188
  23 .7
  16.1
  3.35
Corr. to 7% 02 & 12% C02'
       20.1      19.5
                            RCA#2 APPENDIX B
                                                                            11

-------
FILE NAME - 3IB
RUN # - 31 - Method  17 Train  B  for  PM
LOCATION - Unit 2A Baghouse Outlet  Duct
DATE - 11/16/99 Time: 1521-1646
PROJECT # - 104703.1.002.05.02
Point #

 1
 2
 3
 4
 5
 6
 7
 8
 9
 10
 11
 12
 13
 14
 15
                                   PROG.=VER 06/27/89
                                   11-23-1999  08:58:00
Delta P
(in. H20)
1.500
1.600
1.600
1.500
1.200
1.500
1.600
1.300
1.300
1.600
1.600
1.300
1.700
1.600
1.600
Delta H
(in.
0.
0.
0.
0.
0.
0.
0.
0.
0.
0.
0.
0.
0.
0.
0.
H20)
49
52
52
49
39
49
52
42
42
52
52
42
55
52
52
Stack
(F)
180
180
180
180
179
181
181
180
179
180
179
179
181
179
179
T Meter T
In(F)
56
57
57
58
58
58
58
58
59
59
58
58
58
58
59
Out (F)
56
57
57
58
57
58
58
58
58
59
58
58
58
58
58
Fraction

DRY CATCH
FILTER

Fraction

PROBE RINSE
IMPINGERS
 Final Wt.  Tare Wt.  Blank Wt. Net Wt,
  (g)        (g)        (g)       (g)
0.0000    0.0000    0.0000    0.0000
3.3642    3.3461    0.0000    0.0181
 Final Wt
  (g)        (g)
3.6010    3.6003
0.0000
Tare Wt.    Vol.
           (ml)
         24.7
          0.0
Probe Rinse Blank  (mg/ml)=
Impinger Blank  (mg/ml)=   0.0000
  0.0000
0.0000
  Net Wt,
   (g)
0.0007
0.0000
 12
                                RCA#2 APPENDIX B

-------
FILE NAME  -  32A
RUN #  - 32  - Method  17 Train A for PM
LOCATION - Unit  2A Baghouse Outlet Duct
DATE - 11/17/99  Time: 0854-1013
PROJECT #  -  104703.1.002.05.01

Initial Meter Volume  (Cubic Feet)=         266.519
Final Meter Volume  (Cubic  Feet)=            291.908
Meter Factor=                                 0.996
Final Leak Rate  (cu  ft/min)=                  0.007
Net Meter Volume  (Cubic Feet)=              25.287
Gas Volume  (Dry  Standard Cubic Feet)=       26.412

Barometric Pressure  (in Hg)=                  29.97
Static Pressure  (Inches H20)=                -27.12

Percent Oxygen=                                 4.8
Percent Carbon Dioxide=                        14.7
Moisture Collected  (ml)=                       71.4
Percent Water=                                 11.3

Average Meter Temperature  (F)=                 47
Average Delta H  (in H20)=                      0.46
Average Delta P  (in H20)=                     1.533
Average Stack Temperature  (F)=                 177

Dry Molecular Weight=                         30.54
Wet Molecular Weight=                         29.13

Average Square Root of Delta P (in H20)=     1.1571
% Isokinetic=                                 100.0

Pitot Coefficient=                             0.84
Sampling Time  (Minutes)=                       75.0
Nozzle Diameter  (Inches)=                     0.146
Stack Axis #1  (Inches)=                        57.0
Stack Axis #2  (Inches)=                        66.0
Rectangular Stack
Stack Area  (Square Feet)=                     26.13

Stack Velocity   (Actual, Feet/min)=           4,407
Flow Rate  (Actual, Cubic ft/min)=           115,139
Flow rate  (Standard, Wet, Cubic ft/min)=     89,242
Flow Rate  (Standard, Dry, Cubic ft/min)=     79,162

Particulate Loading - Front Half

Particulate Weight (g)=                      0.0208
Particulate Loading, Dry Std.  (gr/scf)=      0.0121
Particulate Loading, Actual (gr/cu ft)=      0.0083
Emission Rate  (Ib/hr)=                         8.23

No Back Half Analysis
PROG.=VER 06/27/89
11-23-1999  08:58:20
Corr. to 7% 02 & 12% CO2
     0.0105    0.0099
                            RCA#2 APPENDIX B
                                                                            13

-------
                         *  *  METRIC UNITS *  *
FILE NAME  -  32A
RUN #  -  32  -  Method 17  Train A for PM
LOCATION - Unit 2A Baghouse  Outlet Duct
DATE - 11/17/99 Time:  0854-1013
PROJECT  #  -  104703.1.002.05.01

Initial  Meter Volume (Cubic  Meters)=          7.547
Final Meter  Volume (Cubic  Meters)=           8.266
Meter Factor=                                0.996
Final Leak Rate (cu m/min)=                  0.0002
Net Meter Volume (Cubic Meters)=              0.716
Gas Volume  (Dry Standard Cubic Meters)=       0.748

Barometric Pressure (mm Hg)=                   761
Static Pressure (mm H20)=                      -689

Percent  Oxygen=                                4.8
Percent  Carbon  Dioxide=                       14.7
Moisture Collected (ml)=                      71.4
Percent  Water=                                 11.3

Average  Meter Temperature  (C)=                   8
Average  Delta H (mm H20) =                      11.8
Average  Delta P (mm H20)=                      38.9
Average  Stack Temperature  (C) =                  81

Dry Molecular Weight=                         30.54
Wet Molecular Weight=                         29.13

Average  Square  Root of  Delta P (mm H20)=    5.8314
% Isokinetic=                                100.0

Pitot Coefficient=                            0.84
Sampling Time (Minutes)=                      75.0
Nozzle Diameter (mm)=                          3.71
Stack Axis #1 (Meters)=                      1.448
Stack Axis #2 (Meters)=                      1.676
Rectangular  Stack
Stack Area  (Square Meters)=                   2.427

Stack Velocity   (Actual, m/min)=              1,343
.Flow rate  (Actual,  Cubic m/min) =              3,260
Flow rate  (Standard, Wet,  Cubic m/min)=       2,527
Flow rate  (Standard, Dry,  Cubic m/min)=       2,242

Particulate  Loading - Front  Half

Particulate Weight (g)=                     0.0208
Particulate Loading, Dry Std.  (mg/cu  m)=      27.8
Particulate Loading, Actual  (mg/cu m)=         19.1
Emission Rate (kg/hr)=                         3.74

No Back Half  Analysis
PROG.=VER 06/27/89
11-23-1999  08:58:20
Corr. to 7% O2 & 12% C02
       24.0      22.7
 14
                                RCA#2 APPENDIX B

-------
FILE NAME - 32A
RUN # - 32 - Method 17 Train A for PM
LOCATION - Unit 2A Baghouse Outlet Duct
DATE - 11/17/99 Time: 0854-1013
PROJECT # - 104703.1.002.05.01
Point #

 1
 2
 3
 4
 5
 6
 7
 8
 9
 10
 11
 12
 13
 14
 15
 16
 17
 18
 19
 20
 21
 22
 23
 24
 25
                                  PROG.=VER 06/27/89
                                  11-23-1999  08:58:20
Delta P
in. H20)
2.500
2.300
2.000
1.050
0.270
2.300
2.000
2.100
0.780
0.140
2.200
1.900
1.800
0.700
0. 060
2.400
2.100
2.100
0. 870
0.080
2.300
2.400
2.300
1.400
0.270
Delta H
(in. H20)
0.75
0.69
0.60
0.31
0.08
0.70
0 .61
0 .64
0.23
0.04
0.67
0.58
0.55
0.21
0.01
0.73
0 .64
0.64
0.26
0.02
0.70
0.74
0.71
0.43
0 .08
Stack
(F)
177
178
178
178
174
177
175
178
177
178
176
178
178
177
176
177
177
177
177
177
177
177
175
177
178
T
In(F)
40
41
42
43
43
44
44
47
47
48
47
48
50
50
50
49
50
51
53
53
51
53
54
56
56
Meter T
Out (F)
40
41
41
41
42
43
42
43
43
44
44
45
45
45
46
46
46
47
48
48
49
49
49
50
50
Fraction

DRY CATCH
FILTER

Fraction
 Final Wt.  Tare Wt.  Blank Wt.  Net Wt,
  (g)         (g)        (g)       (g)
0.0000    0.0000    0.0000    0.0000
3.3131    3.2944    0.0000    0.0187
 Final Wt.  Tare Wt.
                       (g)        (g)
PROBE RINSE          3.7253     3.7232
IMPINGERS            0.0000     0.0000
Probe Rinse Blank  (mg/ml)=   0.0000
Impinger Blank  (mg/ml)=   0.0000
  Vol
 (ml)
26.7
 0.0
  Net Wt
   (g)
0.0021
0.0000
                            RCA#2 APPENDIX B
                                                                             15

-------
FILE NAME  -  32B
RUN #  -  32  -  Method 17  Train B  for PM
LOCATION - Unit  2A Baghouse  Outlet Duct
DATE - 11/17/99  Time: 0854-1014
PROJECT  #  -  104703.1.002.05.02

Initial  Meter Volume (Cubic  Feet)=         897.879
Final Meter  Volume (Cubic  Feet)=            925.209
Meter Factor=                                1.010
Final Leak Rate  (cu ft/min)=                 0.004
Net Meter Volume (Cubic Feet)=               27.603
Gas Volume  (Dry  Standard Cubic  Feet)=       28.660

Barometric Pressure (in Hg)=                 29.97
Static Pressure  (Inches H20)=                -27.12

Percent  Oxygen=                                 4 . 8
Percent  Carbon Dioxide=                       14.7
Moisture Collected (ml}=                      82.3
Percent  Water=                                 11.9

Average  Meter Temperature  (F)=                   50
Average  Delta H  (in H20)=                      0.44
Average  Delta P  (in H20)=                     1.394
Average  Stack Temperature  (F)=                  180

Dry Molecular Weight=                         30.54
Wet Molecular Weight=                         29.05

Average  Square Root of  Delta P  (in H20)=     1.1780
% Isokinetic=                                100.7

Pitot Coefficient=                            0.84
Sampling Time (Minutes)=                      80.0
Nozzle Diameter  (Inches)=                     0.146
Stack Axis #1 (Inches)=                       57.0
Stack Axis #2 (Inches)=                       66.0
Rectangular  Stack
Stack Area  (Square Feet)=                     26.13

Stack Velocity   (Actual, Feet/min)=          4,502
Flow Rate  (Actual,  Cubic ft/min)=           117,627
.Flow rate  (Standard, Wet,  Cubic ft/min)=     90,790
Flow Rate  (Standard, Dry,  Cubic ft/min)=     79,974

Particulate  Loading - Front  Half

Particulate Weight (g) =                     0.0142
Particulate  Loading, Dry Std.  (gr/scf)=      0.0076
Particulate  Loading, Actual  (gr/cu ft)=      0.0052
Emission Rate (lb/hr)=                         5.23

No Back  Half  Analysis
PROG.=VER 06/27/89
11-23-1999  08:58:30
Corr. to 7% 02 & 12% C02
     0.0066    0.0062
 16
                                RCA#2 APPENDIX B

-------
                        *  * METRIC UNITS  *  *
FILE NAME - 32B
RUN ft - 32 - Method 17 Train B  for PM
LOCATION - Unit 2A Baghouse Outlet Duct
DATE - 11/17/99 Time: 0854-1014
PROJECT # - 104703.1.002.05.02

Initial Meter Volume  (Cubic Meters)=        25.424
Final Meter Volume  (Cubic  Meters)=          26.198
Meter Factor=                                 1.010
Final Leak Rate  (cu m/min)=                 0.0001
Net Meter Volume  (Cubic Meters)=              0.782
Gas Volume (Dry Standard Cubic  Meters)=       0.812

Barometric Pressure  (mm Hg)=                    761
Static Pressure  (mm H20)=                      -689

Percent Oxygen=                                 4.8
Percent Carbon Dioxide=                        14.7
Moisture Collected  (ml}=                       82.3
Percent Water=                                 11.9

Average Meter Temperature  (C)=                   10
Average Delta H  (mm H20)=                      11.1
Average Delta P  (mm H20) =                      35.4
Average Stack Temperature  (C) =                   82

Dry Molecular Weight=                         30.54
Wet Molecular Weight=                         29.05

Average Square Root of Delta P  (mm H20)=    5.9371
% Isokinetic=                                 100.7

Pitot Coefficient=                             0.84
Sampling Time (Minutes)=                       80.0
Nozzle Diameter  (mm)=                          3.71
Stack Axis #1 (Meters)=                       1.448
Stack Axis #2 (Meters)=                       1.676
Rectangular Stack
Stack Area (Square Meters)=                   2.427

Stack Velocity   (Actual, m/min)=              1,372
Flow rate (Actual, Cubic m/min)=              3,331
Flow rate (Standard, Wet,  Cubic m/min)=       2,571
Flow rate (Standard, Dry,  Cubic m/min)=       2,265

Particulate Loading - Front Half

Particulate Weight  (g)=                     0.0142
Particulate Loading, Dry Std.  (mg/cu m)=       17.5
Particulate Loading, Actual  (mg/cu m)=         11.9
Emission Rate (kg/hr)=                         2.37

No Back Half Analysis
PROG.=VER 06/27/89
11-23-1999  08:58:30
Corr. to 7% 02
       15.1
& 12% C02
  14.3
                            RCA#2 APPENDIX B
                                                                            17

-------
FILE NAME - 32B
RUN # - 32 - Method  17  Train  B  for PM
LOCATION - Unit 2A Baghouse Outlet Duct
DATE - 11/17/99 Time: 0854-1014
PROJECT # - 104703.1.002.05.02
'oint #

1
2
3
4
5
6
7
8
9
10
11
12
13
14
15
16
Delta P
(in. H20)
1.300
1.600
1.500
1.200
1.200
1.500
1.400
1.200
1.400
1.700
1.400
1.400
1.300
1.800
1.300
1.100
Delta H
(in. H20)
0.40
0.50
0.47
0.37
0.37
0.47
0.44
0.36
0.44
0.54
0.44
0.44
0.41
0.58
0.41
0.35
Stack
(F)
178
182
179
178
179
179
179
180
181
179
180
180
181
180
178
181
T Meter T
In(F)
43
44
44
45
47
48
50
51
52
54
55
56
51
57
58
60
Out (F)
43
43
43
44
45
46
47
48
48
50
51
52
53
53
54
56
                                   PROG.=VER 06/27/89
                                   11-23-1999  08:58:30
Fraction

DRY CATCH
FILTER

Fraction
PROBE RINSE
IMPINGERS
Probe Rinse Blank  (mg/ml)=
Impinger Blank  (mg/ml)=  0.0000
 Final Wt.  Tare Wt.  Blank Wt. Net Wt,
  (g)        (g)        (g)       (g)
0.0000    0.0000    0.0000    0.0000
3.3168    3.3034    0.0000    0.0134
Final
(g)
.5713
.0000
•/ml) =
Wt



0
. Tare Wt .
(g)
3.5705
0.0000
.0000
Vol.
(ml)
23.9
0.0



0
0

Net Wt
(g)
.0008
.0000

 18
                                RCA#2 APPENDIX B

-------
FILE NAME - 33A
RUN # - 33 - Method 17 Train A  for PM
LOCATION - Unit 2A Baghouse Outlet Duct
DATE - 11/17/99 Time: 1133-1322
PROJECT # - 104703.1.002.05.01

Initial Meter Volume  (Cubic Feet)=         307.184
Final Meter Volume  (Cubic Feet)=           341.362
Meter Factor=                             .   0.996
Final Leak Rate  (cu ft/min)=                 0.001
Net Meter Volume  (Cubic Feet)=              34.041
Gas Volume (Dry Standard Cubic  Feet)=       34.856

Barometric Pressure  (in Hg) =                 30.00
Static Pressure  (Inches H20)=               -26.85

Percent Oxygen=                                3 . 3
Percent Carbon Dioxide=                       15.4
Moisture Collected  (ml)=                     103.9
Percent Water=                                12.3

Average Meter Temperature  (F) =                   57
Average Delta H  (in H20)=                     0.47
Average Delta P  (in H20)=                    1.504
Average Stack Temperature  (F)=                 178

Dry Molecular Weight=                        30.60
Wet Molecular Weight=                        29.05

Average Square Root of Delta P  (in H20)=    1.1403
% Isokinetic=                                101.4

Pitot Coefficient=                            0.84
Sampling Time  (Minutes)=                     100.0
Nozzle Diameter  (Inches)=                    0.146
Stack Axis #1  (Inches)=                       57.0
Stack Axis #2  (Inches)=                       66.0
Rectangular Stack
Stack Area (Square Feet)=                    26.13

Stack Velocity   (Actual, Feet/min)=          4,348
Flow Rate (Actual, Cubic ft/min)=          113,603
Flow rate (Standard, Wet, Cubic ft/min)=    88,092
Flow Rate (Standard, Dry, Cubic ft/min)=    77,247

Particulate Loading - Front Half

Particulate Weight  (g)=                     0.0279
Particulate Loading, Dry Std.  (gr/scf)=     0.0123
Particulate Loading, Actual  (gr/cu ft)=     0.0084
Emission Rate  (lb/hr)=                        8.16

No Back Half Analysis
PROG.=VER 06/27/89
11-23-1999  09:05:16
Corr. to 7% 02
     0.0097
& 12% C02
0.0096
                            RCA#2 APPENDIX B
                                                                            19

-------
                         *  * METRIC UNITS  *  *
FILE NAME - 33A
RUN # - 33 - Method  17 Train A  for PM
LOCATION - Unit 2A Baghouse Outlet Duct
DATE - 11/17/99 Time: 1133-1322
PROJECT # - 104703.1.002.05.01

Initial Meter Volume  (Cubic Meters)=          8.698
Final Meter Volume  (Cubic  Meters)=            9.666
Meter Factor=                                 0.996
Final Leak Rate  (cu m/min)=                 0.0000
Net Meter Volume  (Cubic  Meters)=              0.964
Gas Volume (Dry Standard Cubic  Meters)=       0.987

Barometric Pressure  (mm  Hg)=                    762
Static Pressure  (mm H20)=                      -682

Percent Oxygen=                                 3 . 3
Percent Carbon Dioxide=                        15.4
Moisture Collected  (ml)=                     103.9
Percent Water=                                 12.3

Average Meter Temperature  (C)=                   14
Average Delta H  (mm H20)=                     .11.8
Average Delta P  (mm H20)=                      38.2
Average Stack Temperature  (C)=                   81

Dry Molecular Weight=                         30.60
Wet Molecular Weight=                         29.05

Average Square Root of Delta P  (mm H20)=    5.7468
% Isokinetic=                                 101.4

Pitot Coefficient=                             0.84
Sampling Time  (Minutes)=                     100.0
Nozzle Diameter  (mm)=                          3.71
Stack Axis #1  (Meters)=                       1.448
Stack Axis #2  (Meters)=                       1.676
Rectangular Stack
Stack Area (Square Meters)=                   2.427

Stack Velocity   (Actual, m/min)=              1,325
.Flow rate (Actual, Cubic m/min) =              3,217
Flow rate (Standard, Wet,  Cubic m/min)=       2,494
Flow rate (Standard, Dry,  Cubic m/min)=       2,187

Particulate Loading  - Front Half

Particulate Weight  (g)=                     0.0279
Particulate Loading, Dry Std.  (mg/cu m)=       28.3
Particulate Loading, Actual  (mg/cu m)=        19.2
Emission Rate  (kg/hr)=                         3.70

No Back Half Analysis
PROG.=VER 06/27/89
11-23-1999  09:05:16
Corr. to 7% 02 & 12% C02
       22.4      22.0
 20
                                RCA#2 APPENDIX B

-------
FILE NAME - 33A
RUN # - 33 - Method 17 Train A  for  PM
LOCATION - Unit 2A Baghouse Outlet  Duct
DATE - 11/17/99 Time: 1133-1322
PROJECT # - 104703.1.002.05.01
Point #

 1
 2
 3
 4
 5
 6
 7
 8
 9
 10
 11
 12
 13
 14
 15
 16
 17
 18
 19
 20
 21
 22
 23
 24
 25
                                  PROG.=VER  06/27/89
                                  11-23-1999   09:05:16
Delta P
in
2.
2.
1.
0.
0.
2.
1.
2.
0.
0.
2.
2.
2.
1.
0.
2.
2.
2.
1.
0.
2.
2.
1.
0.
0.
. H20)
200
000
800
620
050
400
800
000
620
120
500
400
400
500
210
300
200
500
050
190
200
100
600
710
140
Delta H
(in.
0.
0.
0.
0.
0.
0.
0.
0.
0.
0.
0.
0.
0.
0.
0.
0.
0.
0.
0.
0.
0.
0.
0.
0.
0.
H20)
67
61
55
19
01
74
56
62
19
03
78
74
75
47
06
72
68
78
33
05
69
65
50
22
04
Stack
(F)
180
181
180
180
180
180
178
177
177
175
174
178
177
175
175
174
180
177
176
177
176
179
179
180
180
T Meter T
In(F)
53
53
55
55
56
55
56
58
59
57
57
58
60
61
62
60
60
62
63
64
61
60
63
64
63
Out (F)
52
52
53
53
53
54
54
54
55
55
55
55
56
56
57
57
57
58
58
58
58
59
59
59
59
Fraction

DRY CATCH
FILTER

Fraction
 Final Wt.  Tare Wt.  Blank Wt. Net Wt,
  (g)        (g)        (g)       (g)
o.oooo    o.oooo    o.oooo    o.oooo
3.3271    3.3016    0.0000    0.0255
 Final Wt
  (g)        (g)
3.6527    3.6503
PROBE RINSE
IMPINGERS           0.0000    0.0000
Probe Rinse Blank  (mg/ml)=  0.0000
Impinger Blank  (mg/ml)=  0.0000
Tare Wt.    Vol.
           (ml)
         23.0
          0.0
  Net Wt,
   (g)
0.0024
0.0000
                            RCA#2 APPENDIX B
                                                                            21

-------
FILE NAME  -  33B
RUN #  -  33  - Method  17  Train B  for  PM
LOCATION - Unit  2A Baghouse  Outlet  Duct
DATE - 11/17/99  Time: 1135-1324
PROJECT  #  -  104703.1.002.05.02

Initial  Meter Volume  (Cubic  Feet)=          940.321
Final Meter Volume (Cubic  Feet)=            974.999
Meter Factor=                                 1.010
Final Leak Rate  (cu  ft/min)=                 0.003
Net Meter Volume (Cubic  Feet)=               35.025
Gas Volume  (Dry  Standard Cubic  Feet)=       35.334

Barometric Pressure  (in  Hg)=                 30.00
Static Pressure  (Inches  H20)=               -26.85

Percent  Oxygen=                                 3 . 3
Percent  Carbon Dioxide=                        15.4
Moisture Collected (ml) =                      98.2
Percent  Water=                                 11.6

Average  Meter Temperature  (F)=                   65
Average  Delta H  (in H20}=                      0.50
Average  Delta P  (in H20)=                     1.553
Average  Stack Temperature  (F)=                  180

Dry Molecular Weight=                         30.60
Wet Molecular Weight=                         29.14

Average  Square Root of Delta P  (in  H20)=     1.1605
% Isokinetic=                                 100.5

Pitot Coefficient=                             0.84
Sampling Time (Minutes)=                     100.0
Nozzle Diameter  (Inches)=                     0.146
Stack Axis #1 (Inches)=                        57.0
Stack Axis #2 (Inches)=                        66.0
Rectangular Stack
Stack Area  (Square Feet)=                     26.13

Stack Velocity   (Actual, Feet/min)=           4,428
Flow Rate  (Actual, Cubic ft/min)=           115,672
Flow rate  (Standard, Wet,  Cubic ft/min)=     89,326
Flow Rate  (Standard, Dry,  Cubic ft/min)=     78,987

Particulate Loading - Front  Half

Particulate Weight  (g)=                      0.0260
Particulate Loading, Dry Std.  (gr/scf)=      0.0113
Particulate Loading, Actual  (gr/cu  ft)=      0.0077
Emission Rate (lb/hr)=                         7.67

No Back Half Analysis
PROG.=VER 06/27/89
11-23-1999  09:05:34
Corr. to 7% O2 & 12% C02
     0.0090    0.0088
 22
                                RCA#2 APPENDIX B

-------
                        * * METRIC UNITS * *
FILE NAME - 33B
RUN # - 33 - Method 17 Train B for PM
LOCATION - Unit 2A Baghouse Outlet Duct
DATE - 11/17/99 Time: 1135-1324
PROJECT # - 104703.1.002.05.02

Initial Meter Volume  (Cubic Meters)=        26.626
Final Meter Volume  (Cubic Meters)=          27.608
Meter Factor=                                1.010
Final Leak Rate (cu m/min)=                 0.0001
Net Meter Volume  (Cubic Meters)=             0.992
Gas Volume (Dry Standard Cubic Meters)=      1.001

Barometric Pressure  (mm Hg)=                   762
Static Pressure (mm H20)=                      -682
PROG.=VER 06/27/89
11-23-1999  09:05:34
Percent Oxygen=                                3.3
Percent Carbon Dioxide=                       15.4
Moisture Collected  (ml)=                      98.2
Percent Water=                                11.6

Average Meter Temperature  (C)=                  18
Average Delta H  (mm H20)=                     12.8
Average Delta P  (mm H20) =                     39.4
Average Stack Temperature  (C)=                  82

Dry Molecular Weight=                        30.60
Wet Molecular Weight=                        29.14

Average Square Root of Delta P  (mm H20)=    5.8487
% Isokinetic=                                100.5

Pitot Coefficient=                            0.84
Sampling Time  (Minutes)=                     100.0
Nozzle Diameter  (mm)=                         3.71
Stack Axis #1  (Meters)=                      1.448
Stack Axis #2  (Meters)=                      1.676
Rectangular Stack
Stack Area (Square Meters)=                  2.427

Stack Velocity   (Actual, m/min)=             1,350
Flow rate  (Actual, Cubic m/min)=             3,275
Flow rate  (Standard, Wet,  Cubic m/min)=      2,529
Flow rate  (Standard, Dry,  Cubic m/min)=      2,237

Particulate Loading - Front Half

Particulate Weight  (g)=                     0.0260
Particulate Loading, Dry Std.  (mg/cu m)=      26.0
Particulate Loading, Actual  (mg/cu m)=        17.7
Emission Rate  (kg/hr)=                        3.48

No Back Half Analysis
Corr. to 7% O2
       20.6
& 12% C02
  20.2
                            RCA#2 APPENDIX B
                                                                            23

-------
FILE NAME - 33B
RUN # - 33 - Method  17 Train B  for  PM
LOCATION - Unit 2A Baghouse Outlet  Duct
DATE - 11/17/99 Time: 1135-1324
PROJECT # - 104703.1.002.05.02
Point #

 1
 2
 3
 4
 5
 6
 7
 8
 9
 10
 11
 12
 13
 14
 15
 16
 17
 18
 19
 20
 21
 22
 23
 24
 25
                                   PROG.=VER 06/27/89
                                   11-23-1999  09:05:34
Delta P
(in. H20)
2.400
2.300
1.900
1.700
0.230
2.300
2.000
1.800
0.830
0.070
2.200
2 .000
1.600
0.640
0 .040
2.200
2.200
2.100
0.760
0.170
2.400
2.700
2.300
1. 800
0.180
Delta H
(in.
0.
0.
0.
0.
0.
0.
0.
0.
0.
0.
0.
0.
0.
0.
0.
0.
0.
0.
0.
0.
0.
0.
0.
0.
0.
H20)
77
74
61
55
07
74
65
58
27
02
72
65
52
21
01
72
72
69
24
05
79
88
75
59
05
Stack
(F)
182
184
183
182
182
181
181
179
178
178
177
180
178
177
179
179
180
179
181
180
180
181
181
184
185
T Meter T
In(F)
61
61
61
62
63
64
64
64
65
66
66
66
66
67
68
68
68
68
69
70
70
69
70
71
72
Out (F)
60
60
60
60
61
62
62
62
63
63
63
64
64
65
65
65
66
66
66
67
67
67
68
68
68
Fraction

DRY CATCH
FILTER

Fraction
 Final Wt.  Tare Wt.  Blank Wt. Net Wt
  (g)        (g)        (g)       (g)
0.0000    0.0000    0.0000    0.0000
3.3350    3.3097    0.0000    0.0253
PROBE RINSE
IMPINGERS
Probe Rinse Blank  (mg/ml)=
 Final Wt.  Tare Wt.    Vol.    Net Wt
  (g)        (g)       (ml)       (g)
3.9072    3.9065    23.3    0.0007
0.0000    0.0000     0.0    0.0000
        0.0000
Impinger Blank  (mg/ml)=  0.0000
 24
                                RCA#2 APPENDK B

-------
FILE NAME - 34A
RUN # - 34 - Method 17 Train A for PM
LOCATION - Unit 2A Baghouse Outlet Duct
DATE - 11/17/99 Time: 1450-1614
PROJECT # - 104703.1.002.05.01

Initial Meter Volume  (Cubic Feet)=         341.752
Final Meter Volume (Cubic Feet)=           368.235
Meter Factor=                                0.996
Final Leak Rate (cu ft/min)=                 0.003
Net Meter Volume  (Cubic Feet)=              26.377
Gas Volume  (Dry Standard Cubic Feet)=       26.738

Barometric Pressure  (in Hg)=                 29.96
Static Pressure (Inches H20)=               -27.39

Percent Oxygen=                                4 . 2
Percent Carbon Dioxide=                       14.6
Moisture Collected (ml)=                      84.5
Percent Water=                                13.0

Average Meter Temperature  (F)=                   62
Average Delta H (in H20)=                     0.49
Average Delta P (in H20) =                    1.577
Average Stack Temperature  (F)=                 179

Dry Molecular Weight=                        30.50
Wet Molecular Weight=                        28.88

Average Square Root of Delta P  (in H20)=    1.1705
% Isokinetic=                                101.7

Pitot Coefficient=                            0.84
Sampling Time  (Minutes)=                      75.0
Nozzle Diameter (Inches)=                    0.146
Stack Axis #1  (Inches)=                       57.0
Stack Axis #2  (Inches)=                       66.0
Rectangular Stack
Stack Area  (Square Feet)=                    26.13

Stack Velocity  (Actual, Feet/min)=          4,487
Flow Rate  (Actual, Cubic ft/min)=          117,221
Flow rate  (Standard, Wet, Cubic  ft/min)=    90,463
Flow Rate  (Standard, Dry, Cubic  ft/min)=    78,742

Particulate Loading  - Front Half

Particulate Weight  (g)=                     0.0116
Particulate Loading, Dry Std.  (gr/scf)=    0.0067
Particulate Loading, Actual  (gr/cu ft)=    0.0045
Emission Rate  (lb/hr)=                        4.51

No Back Half Analysis
PROG.=VER 06/27/89
11-23-1999  09:05:48
Corr. to 7% 02 & 12% C02
     0.0056    0.0055
                            RCA#2 APPENDIX B
                                                                            25

-------
                         *  *  METRIC UNITS * *
 FILE NAME  -  34A
 RUN #  -  34 -  Method 17  Train A for PM
 LOCATION - Unit 2A Baghouse  Outlet Duct
 DATE - 11/17/99 Time:  1450-1614
 PROJECT  #  -  104703.1.002.05.01

 Initial  Meter Volume (Cubic  Meters)=          9.677
 Final Meter Volume (Cubic  Meters)=          10.427
 Meter Factor=                                0.996
 Final Leak Rate (cu m/min)=                  0.0001
 Net Meter Volume (Cubic Meters)=              0.747
 Gas Volume  (Dry Standard Cubic Meters)=      0.757

 Barometric Pressure (mm Hg)=                   761
 Static Pressure (mm H20)=                      -696

 Percent  Oxygen=                                4.2
 Percent  Carbon Dioxide=                       14.6
 Moisture Collected (ml)=                      84.5
 Percent  Water=                                13.0

 Average  Meter Temperature  (C) =                  17
 Average  Delta H (mm H20)=                      12.5
 Average  Delta P (mm H20)=                      40.1
 Average  Stack Temperature  (C)=                  82

 Dry Molecular Weight=                         30.50
 Wet Molecular Weight=                         28.88

 Average  Square Root of  Delta P (mm H20)=    5.8992
 %  Isokinetic=               '                 101.7

 Pitot Coefficient=                            0.84
 Sampling Time (Minutes)=                      75.0
 Nozzle Diameter (mm)=                          3.71
 Stack Axis #1 (Meters)=                      1.448
 Stack Axis #2 (Meters)=                      1.676
 Rectangular Stack
 Stack Area  (Square Meters)=                   2.427

 Stack Velocity  (Actual, m/min)=              1,368
.Flow rate  (Actual,  Cubic m/min)=              3,319
 Flow rate  (Standard, Wet,  Cubic m/min)=      2,562
 Flow rate  (Standard, Dry,  Cubic m/min)=      2,230

 Particulate Loading - Front  Half

 Particulate Weight (g)=                     0.0116
 Particulate Loading, Dry Std.  (mg/cu  m)=      15.3
 Particulate Loading, Actual  (mg/cu m)=        10.3
 Emission Rate (kg/hr)=                         2.05

 No Back  Half  Analysis
PROG.=VER 06/27/89
11-23-1999  09:05:48
Corr. to 7% 02
       12.8
& 12% C02
  12.6
 26
                                RCA#2 APPENDK B

-------
FILE NAME - 34A
RUN # - 34 - Method 17 Train A  for  PM
LOCATION - Unit 2A Baghouse Outlet  Duct
DATE - 11/17/99 Time: 1450-1614
PROJECT # - 104703.1.002.05.01
Point #

 1
 2
 3
 4
 5
 6
 7
 8
 9
 10
 11
 12
 13
 14
 15
 16
 17
 18
 19
 20
 21
 22
 23
 24
 25
                                  PROG.=VER  06/27/89
                                  11-23-1999   09:05:48
Delta P
in. H20)
2.200
2.600
2.200
1.800
0.320
2.200
2.100
2.000
0.850
0.110
2.200
1.900
1.700
0.730
0.030
2.300
2 .200
2.000
0.720
0.120
2.600
2.300
2.300
1.800
0.150
Delta H
(in
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
. H20)
.68
.81
.68
.56
.10
.69
.65
.62
.26
.03
.69
.59
.53
.23
.01
.72
.68
.63
.22
.03
.82
.72
.72
.56
.04
Stack
(F)
180
179
178
180
179
177
181
179
179
178
178
179
179
179
179
179
182
178
178
178
178
180
180
180
179
T Meter T
In(F)
59
58
59
60
61
61
61
62
63
63
63
62
64
66
65
63
63
65
66
66
65
66
68
68
69
Out (F)
58
58
58
58
59
59
59
59
60
60
60
60
60
61
61
61
61
62
62
62
63
63
63
63
63
Fraction

DRY CATCH
FILTER

Fraction
 Final Wt.  Tare Wt. Blank Wt. Net Wt
  (g)        (g)        (g)       (g)
0.0000    0.0000    0.0000    0.0000
3.3081    3.2993    0.0000    0.0088
 Final Wt.  Tare Wt.
                       (g)        (g)
PROBE RINSE          3.7852     3.7824
IMPINGERS            0.0000     0.0000
Probe Rinse Blank  (mg/ml)=   0.0000
Impinger Blank  (mg/ml)=   0.0000
Vol.
                      (mi;
                    21.8
                      0.0
  Net Wt
   (g)
0.0028
0 .0000
                            RCA#2 APPENDIX B
                                                                             27

-------
FILE NAME  - 34B
RUN #  - 34 - Method  17  Train  B  for  PM
LOCATION - Unit  2A Baghouse Outlet  Duct
DATE - 11/17/99  Time: 1450-1615
PROJECT #  - 104703.1.002.05.02

Initial Meter Volume (Cubic Feet)=          978.838
Final Meter Volume  (Cubic  Feet)=           1007.228
Meter Factor=                                 1.010
Final Leak Rate  (cu  ft/min)=                  0.003
Net Meter Volume  (Cubic Feet)=               28.674
Gas Volume (Dry  Standard Cubic  Feet)=        28.895

Barometric Pressure  (in Hg)=                  29.96
Static Pressure  (Inches H20)=               -27.39

Percent Oxygen=                                 4.2
Percent Carbon Dioxide=                       14.6
Moisture Collected  (ml)=                      87.3
Percent Water=                                 12.5

Average Meter Temperature  (F)=                   65
Average Delta H  (in  H20)=                      0.41
Average Delta P  (in  H20)=                     1.262
Average Stack Temperature  (F)=                  182

Dry Molecular Weight=                         30.50
Wet Molecular Weight=                         28.95

Average Square Root  of  Delta  P  (in  H20)=     1.1174
% Isokinetic=                                 101.4

Pitot Coefficient=                             0.84
Sampling Time (Minutes)=                      85.0
Nozzle Diameter  (Inches)=                     0.146
Stack Axis #1 (Inches)=                       57.0
Stack Axis #2 (Inches)=                       66.0
Rectangular Stack
Stack Area (Square Feet)=                     26.13

Stack Velocity   (Actual, Feet/min)=          4,287
Flow Rate  (Actual, Cubic ft/min)=           112,010
.Flow rate  (Standard, Wet,  Cubic ft/min)=     86,083
Flow Rate  (Standard, Dry,  Cubic ft/min)=     75,359

Particulate Loading  - Front Half

Particulate Weight  (g)=                     0.0137
Particulate Loading, Dry Std.  (gr/scf)=      0.0073
Particulate Loading, Actual  (gr/cu  ft)=      0.0049
Emission Rate (lb/hr)=                         4.72

No Back Half Analysis
PROG.=VER 06/27/89
11-23-1999  09:05:58
Corr. to 7% 02 & 12% C02
     0.0061    0.0060
 28
                                RCA#2 APPENDIX B

-------
                        * * METRIC UNITS * *
FILE NAME - 34B
RUN # - 34 - Method 17 Train B for PM
LOCATION - Unit 2A Baghouse Outlet Duct
DATE - 11/17/99 Time: 1450-1615
PROJECT # - 104703.1.002.05.02

Initial Meter Volume  (Cubic Meters)=        27.717
Final Meter Volume  (Cubic Meters)=          28.521
Meter Factor=                                1.010
Final Leak Rate (cu m/min)=                 0.0001
Net Meter Volume  (Cubic Meters)=             0.812
Gas Volume  (Dry Standard Cubic Meters)=      0.818

Barometric Pressure  (mm Hg)=                   761
Static Pressure (mm H20)=                      -696

Percent Oxygen=                                4.2
Percent Carbon Dioxide=                        14.6
Moisture Collected  (ml)=                       87.3
Percent Water=                                 12.5

Average Meter Temperature  (C)=                   18
Average Delta H (mm H20)=                      10.3
Average Delta P (mm H20) =                      32.0
Average Stack Temperature  (C)=                   83

Dry Molecular Weight=                        30.50
Wet Molecular Weight=                        28.95

Average Square Root of Delta P  (mm H20)=    5.6314
% Isokinetic=                                101.4

Pitot Coefficient=                             0.84
Sampling Time  (Minutes)=                       85.0
Nozzle Diameter (mm)=                          3.71
Stack Axis #1  (Meters)=                      1.448
Stack Axis #2  (Meters)=                      1.676
Rectangular Stack
Stack Area  (Square Meters)=                  2.427

Stack Velocity  (Actual, m/min)=             1,307
Flow rate  (Actual, Cubic m/min)=             3,172
Flow rate  (Standard, Wet, Cubic m/min)=      2,438
Flow rate  (Standard, Dry, Cubic m/min)=      2,134

Particulate Loading  - Front Half

Particulate Weight  (g)=                     0.0137
Particulate Loading, Dry Std.  (mg/cu  m)=       16.7
Particulate Loading, Actual  (mg/cu m) =         11.3
Emission Rate  (kg/hr)=                         2.14

No Back Half Analysis
PROG.=VER 06/27/89
11-23-1999  09:05:58
Corr. to  7% O2
       14 .0
& 12% C02
  13 .8
                            RCA#2 APPENDIX B
                                                                            29

-------
FILE NAME - 34B
RUN # - 34 - Method  17  Train B  for PM
LOCATION - Unit  2A Baghouse  Outlet Duct
DATE - 11/17/99  Time: 1450-1615
PROJECT # - 104703.1.002.05.02
Point #

 1
 2
 3
 4
 5
 6
 7
 8
 9
 10
 11
 12
 13
 14
 15
 16
 17
                                                       PROG.=VER 06/27/89
                                                       11-23-1999  09:05:58
Delta P
(in. H20)
1.300
1.200
0.870
1.400
1.400
1.300
0.830
1.400
1.100
1.200
1.200
1.800
1.300
1.000
1.600
1.600
0.950
Delta H
(in.
0.
0.
0.
0.
0.
0.
0.
0.
0.
0.
0.
0.
0.
0.
0.
0.
0.
H20)
42
39
28
45
45
42
26
45
35
39
39
58
42
32
52
52
31
Stack
(F)
182
181
183
181
183
182
182
183
181
181
181
181
181
182
180
181
184
T Meter T
In(F)
63
63
63
63
64
63
64
66
66
66
66
67
68
69
69
70
70
Out (F)
63
63
63
63
63
63
62
63
63
64
64
67
64
65
66
66
67
Fraction

DRY CATCH
FILTER

Fraction
                     Final Wt. Tare Wt.  Blank  Wt.  Net  Wt
                       (g)        (g)        (g)       (g)
                    0.0000    0.0000     0.0000    0.0000
                    3.2867    3.2733     0.0000    0.0134
                     Final Wt
                       (g)        (g)
PROBE RINSE         3.6078    3.6075
IMPINGERS           0.0000    0.0000
Probe Rinse Blank  (mg/ml)=   0.0000
Impinger Blank  (mg/ml)=  0.0000
Tare Wt.    Vol.
           (ml)
         26.8
          0.0
  Net Wt
   (g)
0.0003
0.0000
 30
                                RCA#2 APPENDIX B

-------
FILE NAME - 35A
RUN # - 35 - Method 17 Train A for PM
LOCATION - Unit 2A Baghouse Outlet Duct
DATE - 11/18/99 Time: 0852-1013
PROJECT # - 104703.1.002.05.01

Initial Meter Volume  (Cubic Feet)=         368.652
Final Meter Volume  (Cubic Feet)=           393.401
Meter Factor=                                0.996
Final Leak Rate (cu ft/min)=                 0.002
Net Meter Volume  (Cubic Feet)=              24.650
Gas Volume (Dry Standard Cubic Feet)=       25.758

Barometric Pressure  (in Hg)=                 30.18
Static Pressure (Inches H20) =               -25.00

Percent Oxygen=                                3 . 8
Percent Carbon Dioxide=                       15.0
Moisture Collected  (ml)=                      74.8
Percent Water=                                12.0

Average Meter Temperature  (F)=                   50
Average Delta H (in H20)=                     0.44
Average Delta P (in H20)=                    1.456
Average Stack Temperature  (F)=                 179

Dry Molecular Weight=                        30.55
Wet Molecular Weight=                        29.04

Average Square Root of Delta P  (in H20)=    1.1225
% Isokinetic=                                100.7

Pitot Coefficient=                            0.84
Sampling Time  (Minutes)=                      75.0
Nozzle Diameter (Inches)=                    0.146
Stack Axis #1  (Inches)=                       57.0
Stack Axis #2  (Inches)=                       66.0
Rectangular Stack
Stack Area (Square Feet)=                    26.13

Stack Velocity  (Actual, Feet/min)=          4,261
Flow Rate  (Actual, Cubic ft/min)=          111,323
Flow rate  (Standard, Wet, Cubic ft/min)=    87,122
Flow Rate  (Standard, Dry, Cubic ft/min)=    76,640

Particulate Loading - Front Half

Particulate Weight  (g)=                     0.0144
Particulate Loading, Dry Std.  (gr/scf)=     0.0086
Particulate Loading, Actual  (gr/cu ft)=     0.0059
Emission Rate  (lb/hr)=                        5.65

No Back Half Analysis
                          PROG.=VER  06/27/89
                          11-23-1999   09:06:10
                          Corr.  to  7%  02  & 12%  C02
                                0.0070     0.0069
RCA#2 APPENDIX B
                                                31

-------
                         *  *  METRIC  UNITS  *  *
FILE NAME  - 35A
RUN # - 35 - Method  17  Train A  for  PM
LOCATION - Unit  2A Baghouse  Outlet  Duct
DATE - 11/18/99  Time: 0852-1013
PROJECT #  - 104703.1.002.05.01

Initial Meter Volume (Cubic  Meters)=        10.439
Final Meter Volume  (Cubic  Meters)=          11.140
Meter Factor=                                 0.996
Final Leak Rate  (cu  m/min)=                 0.0001
Net Meter Volume (Cubic Meters)=              0.698
Gas Volume (Dry  Standard Cubic  Meters)=       0.729

Barometric Pressure  (mm Hg)=                   767
Static Pressure  (mm  H20)=                      -635

Percent Oxygen=                                 3 . 8
Percent Carbon Dioxide=                       15.0
Moisture Collected  (ml)=                      74.8
Percent Water=                                 12 . 0

Average Meter Temperature  (C)=                   10
Average Delta H  (mm  H20)=                      11.2
Average Delta P  (mm  H20)=                      37.0
Average Stack Temperature  (C)=                   82

Dry Molecular Weight=                         30.55
Wet Molecular Weight=                         29.04

Average Square Root  of  Delta P  (mm  H20) =    5.6572
% Isokinetic=                                 100.7

Pitot Coefficient=                             0.84
Sampling Time  (Minutes)=                      75.0
Nozzle Diameter  (mm)=                          3.71
Stack Axis #1  (Meters)=                      1.448
Stack Axis #2  (Meters)=                      1.676
Rectangular Stack
Stack Area (Square Meters)=                   2.427

Stack Velocity   (Actual, m/min)=              1,299
.Flow rate  (Actual, Cubic m/min) =              3,152
Flow rate  (Standard, Wet,  Cubic m/min)=       2,467
Flow rate  (Standard, Dry,  Cubic m/min)=       2,170

Particulate Loading  - Front  Half

Particulate Weight  (g)=                    0.0144
Particulate Loading, Dry Std.  (mg/cu  m)=       19.7
Particulate Loading, Actual  (mg/cu  m)=        13.6
Emission Rate  (kg/hr)=                         2.57

No Back Half Analysis
PROG.=VER 06/27/89
11-23-1999  09:06:10
Corr. to 7% 02 & 12% C02
       16.1      15.8
 32
                                RCA#2 APPENDIX B

-------
FILE NAME - 35A
RUN # - 35 - Method 17 Train A  for PM
LOCATION - Unit 2A Baghouse Outlet Duct
DATE - 11/18/99 Time: 0852-1013
PROJECT # - 104703.1.002.05.01
Point #

 1
 2
 3
 4
 5
 6
 7
 8
 9
 10
 11
 12
 13
 14
 15
 16
 17
 18
 19
 20
 21
 22
 23
 24
 25
                                  PROG.=VER 06/27/89
                                  11-23-1999  09:06:10
Delta P
(in. H20)
2.300
2.200
1.800
1.100
0.280
2.200
1.800
1. 900
0.730
0.070
2.200
1.800
1.800
0.700
0. 090
2.300
2.000
1.800
0.810
0.050
2.400
2.500
2.200
1.200
0.170
Delta H
(in
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
. H20)
.69
.66
.54
.33
.08
.67
.54
.58
.22
.02
.67
.55
.55
.21
.02
.71
.61
.55
.25
.01
.74
.77
.68
.37
.05
Stack
(F)
178
179
179
179
178
178
180
180
179
179
178
180
179
180
178
178
180
180
179
178
178
181
180
180
179
T Meter T
In(F)
41
43
44
45
46
46
47
49
50
51
51
51
53
54
55
54
55
57
58
58
58
58
59
61
61
Out (F)
40
41
42
42
43
43
44
45
45
46
46
47
48
49
49
50
50
51
52
52
53
54
54
55
55
Fraction

DRY CATCH
FILTER

Fraction

PROBE RINSE
IMPINGERS
 Final Wt.  Tare Wt.  Blank Wt.  Net Wt
  (g)         (g)        (g)       (g)
0.0000    0.0000    0.0000    0.0000
3.3161    3.3027    0.0000    0.0134
 Final Wt
  (g)
3.6943
0.0000
Probe Rinse Blank  (mg/ml)=   0
 Tare Wt,
  (g)
3.6933
0.0000
0000
  Vol.
 (ml)
27.2
 0.0
  Net Wt
   (g)
0.0010
0.0000
Impinger Blank  (mg/ml)=   0.0000
                            RCA#2 APPENDIX B
                                                                             33

-------
FILE NAME  -  35B
RUN #  - 35  - Method 17  Train  B  for  PM
LOCATION -  Unit  2A Baghouse Outlet  Duct
DATE - 11/18/99  Time: 0853-1013
PROJECT #  -  104703.1.002.05.02

Initial Meter Volume (Cubic Feet)=           14.138
Final Meter  Volume (Cubic  Feet}=             40.414
Meter Factor=                                 1.010
Final Leak  Rate  (cu ft/min)=                  0.003
Net Meter Volume  (Cubic Feet)=               26.539
Gas Volume  (Dry  Standard Cubic  Feet)=       27.751

Barometric  Pressure (in Hg)=                  30.18
Static Pressure  (Inches H20)=               -25.00

Percent Oxygen=                                 3 . 8
Percent Carbon Dioxide=                       15.0
Moisture Collected (ml)=                      75.7
Percent Water=                                 11.4

Average Meter Temperature  (F}=                  50
Average Delta H  (in H20)=                      0.40
Average Delta P  (in H20)=                     1.293
Average Stack Temperature  (F)=                  181

Dry Molecular Weight=                         30.55
Wet Molecular Weight=                         29.12

Average Square Root of  Delta  P  (in  H20)=     1.1337
% Isokinetic=                                 100.3

Pitot Coefficient=                            0.84
Sampling Time  (Minutes)=                      80.0
Nozzle Diameter  (Inches)=                     0.146
Stack Axis  #1  (Inches)=                       57.0
Stack Axis #2  (Inches)=                       66.0
Rectangular  Stack
Stack Area  (Square Feet)=                     26.13

Stack Velocity   (Actual, Feet/min)=   -       4,306
Flow Rate  (Actual,  Cubic ft/min)=           112,484
.Flow rate  (Standard, Wet,  Cubic ft/min)=     87,707
Flow Rate  (Standard, Dry,  Cubic ft/min)=     77,721

Particulate  Loading - Front Half

Particulate  Weight (g)=                     0.0088
Particulate  Loading, Dry Std.  (gr/scf)=      0.0049
Particulate  Loading, Actual  (gr/cu  ft)=      0.0034
Emission Rate  (lb/hr)=                         3.25

No Back Half Analysis
PROG.=VER 06/27/89
11-23-1999  09:06:27
Corr. to 7% 02 & 12% C02
     0.0040    0.0039
 34
                                RCA#2 APPENDIX B

-------
                        * * METRIC UNITS * *
FILE NAME - 35B
RUN # - 35 - Method 17 Train B for PM
LOCATION - Unit 2A Baghouse Outlet Duct
DATE - 11/18/99 Time: 0853-1013
PROJECT # - 104703.1.002.05.02

Initial Meter Volume  (Cubic Meters)=         0.400
Final Meter Volume  (Cubic Meters)=           1.144
Meter Factor=                                1.010
Final Leak Rate  (cu m/min)=                 0.0001
Net Meter Volume  (Cubic Meters)=             0.751
Gas Volume (Dry Standard Cubic Meters)=      0.786

Barometric Pressure  (mm Hg)=                   767
Static Pressure  (mm H20)=                      -635

Percent Oxygen=                                3 . 8
Percent Carbon Dioxide=                        15.0
Moisture Collected  (ml)=                       75.7
Percent Water=                                 11.4

Average Meter Temperature  (C)=                   10
Average Delta H  (mm H20)=                      10.3
Average Delta P  (mm H20)=                      32.8
Average Stack Temperature  (C)=                   83

Dry Molecular Weight=                        30.55
Wet Molecular Weight=                        29.12

Average Square Root of Delta P  (mm H20)=    5.7136
% Isokinetic=                                100.3

Pitot Coefficient=                             0.84
Sampling Time  (Minutes)=                       80.0
Nozzle Diameter  (mm)=                          3.71
Stack Axis #1  (Meters)=                      1.448
Stack Axis #2  (Meters)=                      1.676
Rectangular Stack
Stack Area (Square Meters)=                  2.427

Stack Velocity   (Actual, m/min)=             1,312
Flow rate  (Actual, Cubic m/min)=             3,185
Flow rate  (Standard, Wet, Cubic m/min)=      2,484
Flow rate  (Standard, Dry, Cubic m/min)=      2,201

Particulate Loading - Front Half

Particulate Weight  (g)=                     0.0088
Particulate Loading, Dry Std.  (mg/cu m)=       11.2
Particulate Loading, Actual  (mg/cu m)=         7.7
Emission Rate  (kg/hr)=                         1.48

No Back Half Analysis
PROG.=VER 06/27/89
11-23-1999  09:06:27
Corr. to 7% 02 &. 12% C02
        9.1       9.0
                            RCA#2 APPENDIX B
                                                                            35

-------
FILE NAME - 35B
RUN # - 35 - Method 17 Train B  for  PM
LOCATION - Unit 2A Baghouse Outlet  Duct
DATE - 11/18/99 Time: 0853-1013
PROJECT # - 104703.1.002.05.02
Point #

 1
 2
 3
 4
 5
 6
 7
 8
 9
 10
 11
 12
 13
 14
 15
 16
                                  PROG.=VER 06/27/89
                                  11-23-1999  09:06:27
Delta P
(in. H20)
1.200
1.500
1.300
1.300
1.300
0.780
1.200
1.200
1.200
1.500
1.400
1.300
1.200
1.600
1.500
1.200
Delta H
(in.
0.
0.
0.
0.
0.
0.
0.
0.
0.
0.
0.
0.
0.
0.
0.
0.
H20)
37
47
40
40
40
24
37
37
38
47
44
41
38
51
48
38
Stack
(F)
180
180
180
181
182
181
182
182
182
181
183
182
181
181
183
182
T Meter T
In(F)
43
44
44
45
47
48
49
50
52
53
54
55
56
56
57
58
Out (F)
42
43
43
44
45
46
46
47
49
50
51
53
53
54
55
56
Fraction

DRY CATCH
FILTER

Fraction

PROBE RINSE
IMPINGERS
Probe Rinse Blank
Impinger Blank  (mg/ml)=  0.0000
 Final Wt.  Tare Wt.  Blank Wt. Net Wt,
  (g)        (g)        (g)       (g)
0.0000    0.0000    0.0000    0.0000
3.3168    3.3080    0.0000    0.0088

 Final Wt.  Tare Wt.    Vol.    Net Wt,
  (g)        (g)       (ml)       (g)
3.8241    3.8241    23.7     0.0000
0.0000    0.0000     0.0     0.0000
     =  0.0000
 36
                                RCA#2 APPENDIX B

-------
FILE NAME - 36A
RUN # - 36 - Method 17 Train A for PM
LOCATION - Unit 2A Baghouse Outlet Duct
DATE - 11/18/99 Time: 1105-1224
PROJECT # - 104703.1.002.05.01

Initial Meter Volume  (Cubic Feet)=         393.787
Final Meter Volume  (Cubic Feet)=           418.247
Meter Factor=                                 0.996
Final Leak Rate (cu ft/min)=                  0.003
Net Meter Volume  (Cubic Feet)=              24.362
Gas Volume (Dry Standard Cubic Feet)=       24.832

Barometric Pressure  (in Hg)=                  30.19
Static Pressure (Inches H20)=               -25.91

Percent Oxygen=                                3.8
Percent Carbon Dioxide=                        14.9
Moisture Collected  (ml)=                       69.5
Percent Water=                                 11.6

Average Meter Temperature  (F)=                   63
Average Delta H (in H20)=                      0.42
Average Delta P (in H20)=                     1.365
Average Stack Temperature  (F)=                 179

Dry Molecular Weight=                         30.54
Wet Molecular Weight=                         29.08

Average Square Root of Delta P (in H20)=    1.0837
% Isokinetic=                                 100.3

Pitot Coefficient=                             0.84
Sampling Time (Minutes)=                       75.0
Nozzle Diameter (Inches)=                     0.146
Stack Axis #1 (Inches)=                        57.0
Stack Axis #2 (Inches)=                        66.0
Rectangular Stack
Stack Area (Square Feet)=                     26.13

Stack Velocity  (Actual, Feet/min)=           4,116
Flow Rate (Actual, Cubic ft/min)=          107,535
Flow rate (Standard, Wet, Cubic ft/min)=    83,968
Flow Rate (Standard, Dry, Cubic ft/min)=    74,188

Particulate Loading - Front Half

Particulate Weight  (g)=                     0.0271
Particulate Loading, Dry Std.  (gr/scf)=     0.0168
Particulate Loading, Actual  (gr/cu ft)=     0.0116
Emission Rate (lb/hr)=                        10.69

No Back Half Analysis
PROG.=VER 06/27/89
11-23-1999  09:06:39
Corr. to 7% 02 & 12% C02
     0.0137    0.0135
                            RCA#2 APPENDIX B
                                                                            37

-------
                        * * METRIC UNITS *  *
FILE NAME - 36A
RUN # - 36 - Method 17 Train A for PM
LOCATION - Unit 2A Baghouse Outlet Duct
DATE - 11/18/99 Time: 1105-1224
PROJECT # - 104703.1.002.05.01

Initial Meter Volume  (Cubic Meters)=        11.150
Final Meter Volume  (Cubic Meters)=          11.843
Meter Factor=                                0.996
Final Leak Rate (cu m/min)=                 0.0001
Net Meter Volume  (Cubic Meters)=             0.690
Gas Volume (Dry Standard Cubic Meters)=      0.703

Barometric Pressure (mm Hg)=                   767
Static Pressure (mm H20) =                     -658

Percent Oxygen=                                3.8
Percent Carbon Dioxide=                       14.9
Moisture Collected  (ml)=                      69.5
Percent Water=                                11.6

Average Meter Temperature  (C)=                   17
Average Delta H (mm H20)=                     10.8
Average Delta P (mm H20)=                     34.7
Average Stack Temperature  (C)=                   82

Dry Molecular Weight=                        30.54
Wet Molecular Weight=                        29.08

Average Square Root of Delta P (mm H20)=    5.4617
% Isokinetic=                                100.3

Pitot Coefficients                            0.84
Sampling Time (Minutes)=                      75.0
Nozzle Diameter (mm)=                         3.71
Stack Axis #1 (Meters)=                      1.448
Stack Axis #2 (Meters)=                      1.676
Rectangular Stack
Stack Area (Square Meters)=                  2.427

Stack Velocity  (Actual, m/min)=             1,255
Flow rate (Actual, Cubic m/min)=             3,045
Flow rate (Standard, Wet, Cubic m/min)=      2,378
Flow rate (Standard, Dry, Cubic m/min)=      2,101

Particulate Loading - Front Half

Particulate Weight  (g)=                     0.0271
Particulate Loading, Dry Std.  (mg/cu m)=      38.5
Particulate Loading, Actual  (mg/cu m)=        26.6
Emission Rate (kg/hr)=                        4.85

No Back Half Analysis
PROG.=VER 06/27/89
11-23-1999  09:06:39
Corr. to 7% 02
       31.4
& 12% C02
  31.0
 38
                                RCA#2 APPENDIX B

-------
FILE NAME - 36A
RUN # - 36 - Method 17 Train A for PM
LOCATION - Unit 2A Baghouse Outlet Duct
DATE - 11/18/99 Time: 1105-1224
PROJECT # - 104703.1.002.05.01
Point #

 1
 2
 3
 4
 5
 6
 7
 8
 9
 10
 11
 12
 13
 14
 15
 16
 17
 18
 19
 20
 21
 22
 23
 24
 25
                                                       PROG.=VER 06/27/89
                                                       11-23-1999  09:06:39
Delta P
in
2.
2.
2.
0.
0.
2.
1.
1.
0.
0.
2.
1.
1.
0.
0.
2.
1.
1.
0.
0.
2.
2.
1.
0.
0.
. H20)
200
400
000
890
270
000
900
600
680
090
000
800
600
640
030
200
600
900
750
050
300
500
600
880
240
Delta H
(in
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
. H20)
.68
.74
.62
.27
.08
.62
.59
.50
.21
.02
.63
.56
.50
.20
.01
.69
.50
.60
.23
.01
.72
.79
.50
.28
.07
Stack
(F)
180
181
180
180
180
179
178
180
180
179
178
182
182
181
179
179
180
179
179
177
179
178
178
177
176
T Meter T
In(F)
57
59
59
61
62
61
61
63
64
64
64
64
66
67
66
65
66
68
68
68
66
68
69
70
70
Out (F)
57
58
58
58
59
59
59
60
60
60
61
61
62
62
62
63
63
63
63
64
64
64
65
65
65
Fraction

DRY CATCH
FILTER

Fraction
                     Final Wt. Tare Wt. Blank Wt. Net  Wt
                       (g)        (g)        (g)       (g)
                    0.0000    0.0000    0.0000    0.0000
                    3.3653    3.3398    0.0000    0.0255
                     Final Wt. Tare Wt.   Vol.    Net  Wt
                       (g)        (g)       (ml)       (g)
PROBE RINSE         3.8339    3.8323     31.6     0.0016
IMPINGERS           0.0000    0.0000      0.0     0.0000
Probe Rinse Blank  (mg/ml)=  0.0000
Impinger Blank  (mg/ml)=  0.0000
                            RCA#2 APPENDIX B
                                                                            39

-------
FILE NAME - 36B
RUN # - 36 - Method 17 Train B for PM
LOCATION - Unit 2A Baghouse Outlet Duct
DATE - 11/18/99 Time: 1105-1225
PROJECT # - 104703.1.002.05.02

Initial Meter Volume  (Cubic Feet)=          40.759
Final Meter Volume  (Cubic Feet)=            66.777
Meter Factor=                                1.010
Final Leak Rate (cu ft/min)=                 0.004
Net Meter Volume  (Cubic Feet)=              26.278
Gas Volume (Dry Standard Cubic Feet)=       26.769

Barometric Pressure (in Hg)=                 30.19
Static Pressure (Inches H20) =               -25.91

Percent Oxygen=                                3 . 3
Percent Carbon Dioxide=                       14.9
Moisture Collected  (ml)=                      81.5
Percent Water=                                12.5

Average Meter Temperature  (F)=                   63
Average Delta H (in H20)=                     0.39
Average Delta P (in H20)=                    1.210
Average Stack Temperature  (F)=                 182

Dry Molecular Weight=                        30.54
Wet Molecular Weight=                        28.96

Average Square Root of Delta P (in H20)=    1.0961
% Isokinetic=                                101.2

Pitot Coefficient=                            0.84
Sampling Time (Minutes)=                      80.0
Nozzle Diameter (Inches)=                    0.146
Stack Axis #1 (Inches)=                       57.0
Stack Axis #2 (Inches)=                       66.0
Rectangular Stack
Stack Area (Square Feet)=                    26.13

Stack Velocity  (Actual,  Feet/min)=          4,179
Flow Rate (Actual, Cubic ft/min)=          109,175
Flow rate (Standard, Wet, Cubic ft/min)=    84,940
Flow Rate (Standard, Dry, Cubic ft/min)=    74,287

Particulate Loading - Front Half

Particulate Weight  (g)=                     0.0171
Particulate Loading, Dry Std. (gr/scf)=     0.0098
Particulate Loading, Actual  (gr/cu ft)=     0.0067
Emission Rate (lb/hr)=                        6.26

No Back Half Analysis
PROG.=VER 06/27/89
11-23-1999  09:06:51
Corr. to 7% 02 & 12% C02
     0.0080    0.0079
 40
                                RCA#2 APPENDIX B

-------
                         *  * METRIC  UNITS  *  *
FILE NAME  - 36B
RUN # - 36 - Method  17 Train  B  for  PM
LOCATION - Unit 2A Baghouse Outlet  Duct
DATE - 11/18/99 Time: 1105-1225
PROJECT #  - 104703.1.002.05.02

Initial Meter Volume  (Cubic Meters)=          1.154
Final Meter Volume  (Cubic  Meters)=            1.891
Meter Factor=                                 1.010
Final Leak Rate  (cu m/min)=                 0.0001
Net Meter Volume  (Cubic  Meters)=              0.744
Gas Volume (Dry Standard Cubic Meters)=       0.758

Barometric Pressure  (mm  Hg)=                    767
Static Pressure  (mm H20)=                      -658

Percent Oxygen=                                 3 . 8
Percent Carbon Dioxide=                        14.9
Moisture Collected  (ml)=                      81.5
Percent Water=                                 12.5

Average Meter Temperature  (C)=                   17
Average Delta H  (mm H20)=                       9.9
Average Delta P  (mm H20)=                      30.7
Average Stack Temperature  (C)=                   83

Dry Molecular Weight=                         30.54
Wet Molecular Weight=                         28.96

Average Square Root of Delta  P  (mm  H20)=    5.5243
% Isokinetic=                                 101.2

Pitot Coefficient=                             0.84
Sampling Time  (Minutes)=                      80.0
Nozzle Diameter  (mm)=                          3.71
Stack Axis #1  (Meters)=                       1.448
Stack Axis #2  (Meters)=                       1.676
Rectangular Stack
Stack Area (Square Meters)=                   2.427

Stack Velocity "(Actual, m/min)=              1,274
Flow rate  (Actual, Cubic m/min)=              3,091
Flow rate  (Standard, Wet,  Cubic m/min)=       2,405
Flow rate  (Standard, Dry,  Cubic m/min)=       2,104

Particulate Loading - Front Half

Particulate Weight  (g)=                     0.0171
Particulate Loading, Dry Std.  (mg/cu m)=       22.6
Particulate Loading, Actual  (mg/cu  m)=         15.3
Emission Rate  (kg/hr)=                         2.84

No Back Half Analysis
PROG.=VER 06/27/89
11-23-1999  09:06:51
Corr. to 7% O2 & 12% CO2
       18.4      18.2
                            RCA#2 APPENDIX B
                                                                            41

-------
FILE NAME - 36B
RUN # - 36 - Method  17 Train B  for  PM
LOCATION - Unit 2A Baghouse Outlet  Duct
DATE - 11/18/99 Time: 1105-1225
PROJECT # - 104703.1.002.05.02
Point #

 1
 2
 3
 4
 5
 6
 7
 8
 9
 10
 11
 12
 13
 14
 15
 16
                                   PROG.=VER 06/27/89
                                   11-23-1999  09:06:51
Delta P
in. H20)
1.300
1.200
1.200
0.860
1.300
1.100
1.300
0 .870
1.300
1.300
0.930
1.300
1.000
1.500
1.400
1.500
Delta H
(in. H20)
0.41
0.38
0.38
0.27
0.42
0.35
0.42
0.28
0.42
0.42
0.30
0.42
0.32
0.49
0.46
0.49
Stack
(F)
183
182
182
182
182
182
182
183
184
182
182
181
180
179
180
179
T Meter T
In(F)
59
59
60
61
62
62
63
64
65
65
66
67
68
68
69
69
Out (F)
58
58
59
59
60
61
61
62
63
64
64
65
65
66
66
67
Fraction

DRY CATCH
FILTER

Fraction

PROBE RINSE
IMPINGERS
Probe Rinse Blank  (mg/ml)=
Impinger Blank  (mg/ml)=  0.0000
 Final Wt.  Tare Wt.  Blank Wt. Net Wt
  (g)        (g)        (g)       (g)
0.0000    0.0000    0.0000    0.0000
3.3951    3.3780    0.0000    0.0171
Final
(g)
3.8595
0.0000
g/ml)=
Wt


0
. Tare Wt .
(g)
3 .8595
0.0000
.0000
Vol.
(ml)
25.4
0.0


0
0

Net Wt
(g)
.0000
.0000

 42
                                RCA#2 APPENDIX B

-------
FILE NAME - 37A
RUN # - 37 - Method 17 Train A  for  PM
LOCATION - Unit 2A Baghouse Outlet  Duct
DATE - 11/18-19/99 Time: 2324-0043
PROJECT # - 104703.1.002.05.01

Initial Meter Volume  (Cubic Feet)=         418.645
Final Meter Volume  (Cubic Feet)=           440.240
Meter Factor=                                 0.996
Final Leak Rate  (cu f t/min) =                  0.001
Net Meter Volume  (Cubic Feet)=              21.509
Gas Volume (Dry Standard Cubic  Feet)=       22.534

Barometric Pressure  (in Hg) =                  30.20
Static Pressure  (Inches H20)=               -17.09
        PROG.=VER 06/27/89
        11-23-1999  09:14:43
Percent Oxygen=
Percent Carbon Dioxide=
Moisture Collected  (ml}=
Percent Water=
 6 . 1
13.5
56
10
                                                  1
                                                  5
Average Meter Temperature  (F) =                  49
Average Delta H  (in H20)=                     0.34
Average Delta P(inH20)=                    1.070
Average Stack Temperature  (F) =                 177

Dry Molecular Weight=                        30.40
Wet Molecular Weight=                        29.10

Average Square Root of Delta P  (in H20)=    0.9635
% Isokinetic=                                 99.7

Pitot Coefficient=                            0.84
Sampling Time (Minutes) =                      75.0
Nozzle Diameter  (Inches) =                    0.146
Stack Axis #1 (Inches) =                       57.0
Stack Axis #2 ( Inches) =                       66.0
Rectangular Stack
Stack Area (Square Feet)=                    26.13

Stack Velocity   (Actual, Feet/min) =          3,609
Flow Rate  (Actual, Cubic f t/min) =           94,290
Flow rate  (Standard, Wet, Cubic f t/min) =    75,633
Flow Rate  (Standard, Dry, Cubic f t/min) =    67,695

Particulate Loading - Front Half

Particulate Weight  (g) =                     0.0512
Particulate Loading, Dry Std.  (gr/scf)=     0.0350
Particulate Loading, Actual  (gr/cu ft)=     0.0251
Emission Rate (lb/hr)=                       20.30

No Back Half Analysis
        Corr. to 7% 02 & 12% C02
             0.0329    0.0311
                            RCA#2 APPENDIX B
                                                                            43

-------
                        * * METRIC UNITS  *  *
FILE NAME - 37A
RUN # - 37 - Method 17 Train A for PM
LOCATION - Unit 2A Baghouse Outlet Duct
DATE - 11/18-19/99 Time: 2324-0043
PROJECT # - 104703.1.002.05.01

Initial Meter Volume  (Cubic Meters)=
Final Meter Volume  (Cubic Meters)=
Meter Factor=
Final Leak Rate (cu m/min)=
Net Meter Volume  (Cubic Meters)=
Gas Volume (Dry Standard Cubic Meters)=

Barometric Pressure (mm Hg)=
Static Pressure (mm H20)=

Percent Oxygen=
Percent Carbon Dioxide=
Moisture Collected  (ml)=
Percent Water=
          PROG.=VER 06/27/89
          11-23-1999  09:14:43
Average Meter Temperature  (C)=
Average Delta H  (mm H20)=
Average Delta P  (mm H20)=
Average Stack Temperature  (C)=

Dry Molecular Weight=
Wet Molecular Weight=

Average Square Root of Delta P  (mm H20)=
% Isokinetic=

Pitot Coefficient=
Sampling Time (Minutes)=
Nozzle Diameter  (mm)=
Stack Axis #1 (Meters)=
Stack Axis #2 (Meters)=
Rectangular Stack
Stack Area (Square Meters)=

Stack Velocity   (Actual, m/min)=
Flow rate  (Actual, Cubic m/min)=
Flow rate  (Standard, Wet,  Cubic m/min)=
Flow rate  (Standard, Dry,  Cubic m/min)=

Particulate Loading - Front Half

Particulate Weight  (g)=
Particulate Loading, Dry Std.  (mg/cu m)=
Particulate Loading, Actual  (mg/cu m)=
Emission Rate (kg/hr)=

No Back Half Analysis
11.854
12.466
 0.996
0.0000
 0.609
 0.638

   767
  -434

   6.1
  13.5
  56.1
  10.5

     9
   8.5
  27.2
    80

 30.40
 29.10

4.8560
  99.7

  0.84
  75.0
  3 .71
 1.448
 1.676

 2.427

 1,100
 2,670
 2,142
 1,917
0.0512
  80.2
  57.6
  9.22
Corr. to 7% 02 & 12% C02
       75.4      71.3
 44
                                RCA#2 APPENDIX B

-------
FILE NAME - 37A
RUN # - 37 - Method 17 Train A  for PM
LOCATION - Unit 2A Baghouse Outlet Duct
DATE - 11/18-19/99 Time: 2324-0043
PROJECT # - 104703.1.002.05.01
Point #

 1
 2
 3
 4
 5
 6
 7
 8
 9
 10
 11
 12
 13
 14
 15
 16
 17
 18
 19
 20
 21
 22
 23
 24
 25
                                                       PROG.=VER 06/27/89
                                                       11-23-1999  09:14:43
Delta P
(in. H20)
1.700
1.600
1.400
0.770
0.140
1.600
1.400
1.400
0.540
0.080
1.400
1.300
1.100
0.420
0. 070
1.700
1.400
1.500
0.520
0. 080
1.800
1.800
1.600
1.300
0.120
Delta H
(in. H20)
0.54
0.50
0.44
0.24
0.04
0.50
0.44
0.44
0.17
0.02
0.44
0.41
0.35
0.13
0.02
0.54
0.44
0.47
0.16
0.02
0.57
0.57
0.51
0.41
0.03
Stack
(F)
177
178
176
177
176
176
177
177
177
176
176
177
177
177
176
177
177
178
178
177
177
177
178
178
172
T Meter T
In(F)
48
47
47
47
48
47
48
49
49
49
49
49
50
51
51
50
50
52
53
52
50
51
52
53
53
Out (F)
47
47
47
47
47
47
47
47
47
48
48
48
48
48
48
48
48
49
49
49
49
49
49
49
50
Fraction

DRY CATCH
FILTER

Fraction
                     Final Wt. Tare Wt. Blank Wt.  Net  Wt
                       (g)        (g)        (g)       (g)
                    0.0000    0.0000    0.0000     0.0000
                    3.4202    3.3734    0.0000     0.0468
                     Final Wt. Tare Wt.   Vol.     Net  Wt.
                       (g)        (g)       (ml)       (g)
PROBE RINSE         3.4512    3.4468     35.7     0.0044
IMPINGERS           0.0000    0.0000      0.0     0.0000
Probe Rinse Blank  (mg/ml)=  0.0000
Impinger Blank  (mg/ml)=  0.0000
                            RCA#2 APPENDIX B
                                                                             45

-------
FILE NAME  -  37B
RUN #  -  37  -  Method  17  Train  B  for  PM
LOCATION - Unit  2A Baghouse Outlet  Duct
DATE - 11/18-19/99 Time:  2324-0044
PROJECT  #  -  104703.1.002.05.02

Initial  Meter Volume  (Cubic Feet)=           76.934
Final Meter Volume  (Cubic Feet)=             98.720
Meter Factor=                                1.010
Final Leak Rate  (cu  ft/min)=                  0.003
Net Meter Volume (Cubic Feet)=               22.004
Gas Volume  (Dry  Standard  Cubic  Feet)=        23.021

Barometric Pressure  (in Hg)=                  30.20
Static Pressure  (Inches H20)=               -17.09

Percent  Oxygen=                                 6 .1
Percent  Carbon Dioxide=                       13.5
Moisture Collected  (ml)=                       53.1
Percent  Water=                                  9.8

Average  Meter Temperature (F}=                   50
Average  Delta H  (in H20)=                     0.27
Average  Delta P  (in H20)=                    0.833
Average  Stack Temperature (F)=                  179

Dry Molecular Weight=                         30.40
Wet Molecular Weight=                         29.19

Average  Square Root of  Delta  P  (in  H20) =     0.9112
% Isokinetic=                                100.6

Pitot Coefficient=                             0.84
Sampling Time (Minutes)=                       80.0
Nozzle Diameter  (Inches)=                    0.146
Stack Axis #1 (Inches)=                       57.0
Stack Axis #2 (Inches)=                       66.0
Rectangular Stack
Stack Area  (Square Feet)=                    26.13

Stack Velocity   (Actual,  Feet/min)=          3,415
Flow Rate  (Actual, Cubic  ft/min)=            89,219
.Flow rate  (Standard, Wet,  Cubic ft/min)=     71,280
Flow Rate  (Standard, Dry,  Cubic ft/min)=     64,295

Particulate Loading  - Front Half

Particulate Weight  (g) =                     0.0333
Particulate Loading, Dry  Std.  (gr/scf)=      0.0223
Particulate Loading, Actual  (gr/cu  ft)=      0.0160
Emission Rate (lb/hr)=                        12.27

No Back  Half  Analysis
PROG.=VER 06/27/89
11-23-1999  09:14:57
Corr. to 7% 02 & 12% C02
     0.0209    0.0198
 46
                                RCA#2 APPENDDC B

-------
                        * * METRIC UNITS * *
FILE NAME - 37B
RUN # - 37 - Method 17 Train B for PM
LOCATION - Unit 2A Baghouse Outlet Duct
DATE - 11/18-19/99 Time: 2324-0044
PROJECT # - 104703.1.002.05.02

Initial Meter Volume  (Cubic Meters)=         2.178
Final Meter Volume (Cubic Meters)=           2.795
Meter Factor=                                1.010
Final Leak Rate (cu m/min)=                 0.0001
Net Meter Volume  (Cubic Meters)=             0.623
Gas Volume (Dry Standard Cubic Meters)=      0.652

Barometric Pressure (mm Hg)=                   767
Static Pressure (mm H20)=                      -434

Percent Oxygen=                                6 .1
Percent Carbon Dioxide=                        13.5
Moisture Collected (ml)=                       53.1
Percent Water=                                 9 . 8

Average Meter Temperature  (C)=                   10
Average Delta H (mm H20)=                      7.0
Average Delta P (mm H20) =                      21.2
Average Stack Temperature  (C)=                   82

Dry Molecular Weight=                        30.40
Wet Molecular Weight=                        29.19

Average Square Root of Delta P  (mm H20)=    4.5925
% Isokinetic=                                100.6

Pitot Coefficient=                             0.84
Sampling Time (Minutes)=                       80.0
Nozzle Diameter (mm)=                          3.71
Stack Axis #1 (Meters)=                      1.448
Stack Axis #2 (Meters)=                      1.676
Rectangular Stack
Stack Area (Square Meters)=                  2.427

Stack Velocity  (Actual, m/min)=             1,041
Flow rate (Actual, Cubic m/min)=             2,526
Flow rate (Standard,  Wet, Cubic m/min)=      2,018
Flow rate (Standard,  Dry, Cubic m/min)=      1,821

Particulate Loading - Front Half

Particulate Weight (g)=                     0.0333
Particulate Loading,  Dry Std.  (mg/cu m)=       51.1
Particulate Loading,  Actual  (mg/cu m)=         36.8
Emission Rate (kg/hr)=                         5.57

No Back Half Analysis
PROG.=VER 06/27/89
11-23-1999  09:14:57
Corr. to 7% O2 & 12% C02
       48.0      45.4
                            RCA#2 APPENDIX B
                                                                            47

-------
FILE NAME - 37B
RUN ft - 37 - Method 17 Train B for PM
LOCATION - Unit 2A Baghouse Outlet Duct
DATE - 11/18-19/99 Time: 2324-0044
PROJECT # - 104703.1.002.05.02
Point #

 1
 2
 3
 4
 5
 6
 7
 8
 9
 10
 11
 12
 13
 14
 15
 16
                                  PROG.=VER  06/27/89
                                  11-23-1999   09:14:57
Delta P
(in
0 .
0.
0 .
0.
0.
0.
0.
0.
0.
0.
0.
0.
0 .
0.
0.
0 .
. H20)
910
840
870
870
940
860
830
800
770
820
650
890
820
950
910
600
Delta H
(in.
0.
0.
0.
0.
0.
0.
0.
0.
0.
0.
0.
0.
0.
0.
0.
0.
H20)
30
28
29
29
31
28
27
26
25
27
21
30
27
32
30
20
Stack
(F)
180
179
180
179
180
179
179
180
179
179
180
178
180
179
179
179
T Meter T
In(F)
48
48
48
48
48
49
49
49
50
50
50
51
52
52
53
53
Out (F)
48
48
48
48
48
48
49
49
49
49
49
50
51
51
51
51
Fraction

DRY CATCH
FILTER

Fraction
PROBE RINSE
IMPINGERS
Probe Rinse Blank  (mg/ml)=
Impinger Blank  (mg/ml)=   0.0000
 Final Wt.  Tare Wt. Blank Wt. Net Wt
  (g)        (g)        (g)       (g)
0.0000    0.0000    0.0000    0.0000
3.3931    3.3611    0.0000    0.0320
Final Wt
(g)
.8260
.0000
7ml )= 0
. Tare Wt .
(g)
3.8247
0.0000
.0000
Vol.
(ml)
29.9
0.0

Net Wt
(g)
0.0013
0.0000

 48
                                 RCA#2 APPENDIX B

-------
FILE NAME  -  38A
RUN #  -  38  - Method  17  Train A for PM
LOCATION -  Unit 2A Baghouse  Outlet Duct
DATE - 11/19/99 Time: 0137-0256
PROJECT  #  -  104703.1.002.05.01

Initial  Meter Volume  (Cubic  Feet)=         440.664
Final Meter  Volume  (Cubic  Feet)=            462.344
Meter Factor=                                 0.996
Final Leak  Rate (cu  ft/min)=                 0.003
Net Meter Volume (Cubic Feet)=              21.593
Gas Volume  (Dry Standard Cubic Feet)=       22.620

Barometric  Pressure  (in Hg)=                 30.20
Static Pressure (Inches H20)=               -17.08

Percent  Oxygen=                                5 . 7
Percent  Carbon  Dioxide=                       13.0
Moisture Collected  (ml)=                      61.7
Percent  Water=                                 11.4

Average  Meter Temperature  (F}=                 49
Average  Delta H (in H20)=                      0.34
Average  Delta P(inH20)=                     1.066
Average  Stack Temperature  (F)=                 177

Dry Molecular Weight=                         30.31
Wet Molecular Weight=                         28.91

Average  Square  Root of  Delta P (in H20)=     0.9565
% Isokinetic=                                 101.6

Pitot Coefficient=                             0.84
Sampling Time  (Minutes)=                      75.0
Nozzle Diameter (Inches)=                     0.146
Stack Axis #1  (Inches)=                       57.0
Stack Axis #2  (Inches)=                       66.0
Rectangular Stack
Stack Area  (Square Feet)=                     26.13

Stack Velocity   '(Actual, Feet/min) =          3,597
Flow Rate  (Actual, Cubic ft/min)=            93,959
Flow rate  (Standard, Wet,  Cubic ft/min)=     75,308
Flow Rate  (Standard, Dry,  Cubic ft/min)=     66,734

Particulate Loading - Front  Half

Particulate Weight  (g)=                     0.0331
Particulate Loading, Dry Std.  (gr/scf)=      0.0225
Particulate Loading, Actual  (gr/cu ft)=      0.0160
Emission Rate  (lb/hr)=                        12.89

No Back Half Analysis
PROG.=VER 06/27/89
11-23-1999  09:15:15
Corr. to 7% 02 & 12% C02
     0.0206    0.0208
                            RCA#2 APPENDIX B
                                                                            49

-------
                        * * METRIC UNITS  *  *
FILE NAME - 38A
RUN # - 38 - Method 17 Train A for PM
LOCATION - Unit 2A Baghouse Outlet Duct
DATE - 11/19/99 Time: 0137-0256
PROJECT # - 104703.1.002.05.01

Initial Meter Volume  (Cubic Meters)=        12.478
Final Meter Volume  (Cubic Meters)=          13.092
Meter Factor=                                 0.996
Final Leak Rate (cu m/min)=                 0.0001
Net Meter Volume  (Cubic Meters)=              0.611
Gas Volume (Dry Standard Cubic Meters)=       0.640

Barometric Pressure  (mm Hg)=                   767
Static Pressure (mm H20)=                      -434

Percent Oxygen=                                5 . 7
Percent Carbon Dioxide=                        13.0
Moisture Collected  (ml)=                       61.7
Percent Water=                                 11.4

Average Meter Temperature  (C)=                   9
Average Delta H (mm H20)=                      8.7
Average Delta P (mm H20)=                      27.1
Average Stack Temperature  (C)=                   81

Dry Molecular Weight=                         30.31
Wet Molecular Weight=                         28.91

Average Square Root of Delta P  (mm H20)=    4.8208
% Isokinetic=                                 101.6

Pitot Coefficient=                             0.84
Sampling Time  (Minutes)=                       75.0
Nozzle Diameter (mm)=                          3.71
Stack Axis #1  (Meters)=                       1.448
Stack Axis #2  (Meters)=                       1.676
Rectangular Stack
Stack Area (Square Meters)=                   2.427

Stack Velocity  (Actual, m/min)=              1,096
Flow rate (Actual, Cubic m/min)=              2,661
Flow rate (Standard, Wet, Cubic m/min)=       2,132
Flow rate (Standard, Dry, Cubic m/min)=       1,890

Particulate Loading - Front Half

Particulate Weight  (g)=                     0.0331
Particulate Loading, Dry Std.  (mg/cu m)=       51.7
Particulate Loading, Actual  (mg/cu m)=         36.7
Emission Rate  (kg/hr)=                         5.85

No Back Half Analysis
PROG.=VER 06/27/89
11-23-1999  09:15:15
Corr. to 7% 02
       47.3
& 12% C02
  47.7
 50
                                RCA#2 APPENDIX B

-------
FILE NAME - 38A
RUN # - 38 - Method 17 Train A for  PM
LOCATION - Unit 2A Baghouse Outlet  Duct
DATE - 11/19/99 Time: 0137-0256
PROJECT # - 104703.1.002.05.01
Point #

 1
 2
 3
 4
 5
 6
 7
 8
 9
 10
 11
 12
 13
 14
 15
 16
 17
 18
 19
 20
 21
 22
 23
 24
 25
                                  PROG.=VER  06/27/89
                                  11-23-1999   09:15:15
Delta P
in. H20)
1.700
1.700
1.600
0.820
0.140
1.600
1.400
1.300
0.560
0.070
1.600
1.400
1.200
0.400
0.030
1.600
1.500
1.400
0.580
0.050
1.700
1.800
1.200
1.200
0.100
Delta H
(in
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
. H20)
.55
.55
.51
.26
.04
.52
.45
.42
.18
.02
.52
.45
.39
.13
.01
.52
.49
.45
.18
.01
.55
.58
.39
.39
.03
Stack
(F)
177
178
179
178
176
178
178
178
177
177
174
178
177
179
177
177
177
177
178
176
177
177
178
177
177
T Meter T
In(F)
48
47
48
49
49
49
5-0
50
51
50
50
50
50
51
51
50
50
52
52
52
50
50
51
53
52
Out (F)
48
47
47
47
47
47
48
47
48
48
48
47
47
48
48
48
48
48
48
48
48
48
48
49
49
Fraction

DRY CATCH
FILTER

Fraction

PROBE RINSE
IMPINGERS
 Final Wt.  Tare Wt.  Blank Wt.  Net Wt,
  (g)        (g)        (g)       (g)
0.0000    0.0000    0.0000    0.0000
3.3855    3.3564    0.0000    0.0291
 Final Wt
  (g)
3 .3977
0.0000
 Tare Wt
  (g)
3.3937
0.0000
Probe Rinse Blank  (mg/ml)=  0.0000
Impinger Blank  (mg/ml)=  0.0000
  Vol
 (ml)
26.2
 0.0
  Net Wt
   (g)
0.0040
0.0000
                            RCA#2 APPENDIX B
                                                                            51

-------
FILE NAME - 38B
RUN # - 38 - Method 17 Train B for PM
LOCATION - Unit 2A Baghouse Outlet Duct
DATE - 11/19/99 Time: 0137-0257
PROJECT # - 104703.1.002.05.02

Initial Meter Volume  (Cubic Feet)=          99.002
Final Meter Volume  (Cubic Feet)=           121.140
Meter Factor=                                1.010
Final Leak Rate (cu ft/min)=                 0.002
Net Meter Volume  (Cubic Feet)=              22.359
Gas Volume (Dry Standard Cubic Feet)=       23.379

Barometric Pressure (in Hg)=                 30.20
Static Pressure (Inches H20)=               -17.08

Percent Oxygen=                                5 . 7
Percent Carbon Dioxide=                       13.0
Moisture Collected  (ml)=                      55.6
Percent Water=                                10.1

Average Meter Temperature  (F)=                   50
Average Delta H (in H20)=                     0.29
Average Delta P (in H20)=                    0.862
Average Stack Temperature  (F)=                 180

Dry Molecular Weight=                        30.31
Wet Molecular Weight=                        29.07

Average Square Root of Delta P (in H20}=    0.9280
% Isokinetic=                                100.4

Pitot Coefficient=                            0.84
Sampling Time (Minutes)=                      80.0
Nozzle Diameter (Inches)=                    0.146
Stack Axis #1 (Inches)=                       57.0
Stack Axis #2 (Inches)=                       66.0
Rectangular Stack
Stack Area (Square Feet)=                    26.13

Stack Velocity  (Actual, Feet/min)=          3,486
Flow Rate (Actual, Cubic ft/min)=           91,065
Flow rate (Standard, Wet, Cubic ft/min)=    72,735
Flow Rate (Standard, Dry, Cubic ft/min)=    65,408

Particulate Loading - Front Half

Particulate Weight  (g)=                     0.0222
Particulate Loading, Dry Std.  (gr/scf)=     0.0146
Particulate Loading, Actual  (gr/cu ft)=     0.0105
Emission Rate (lb/hr)=                        8.20

No Back Half Analysis
PROG.=VER 06/27/89
11-23-1999  09:15:26
Corr. to 7% 02 & 12% C02
     0.0134    0.0135
 52
                                RCA#2 APPENDIX B

-------
                        * * METRIC UNITS * *
FILE NAME - 38B
RUN # - 38 - Method 17 Train B for PM
LOCATION - Unit 2A Baghouse Outlet Duct
DATE - 11/19/99 Time: 0137-0257
PROJECT # - 104703.1.002.05.02

Initial Meter Volume  (Cubic Meters)=         2.803
Final Meter Volume (Cubic Meters)=           3.430
Meter Factor=                                1.010
Final Leak Rate (cu m/min)=                 0.0001
Net Meter Volume  (Cubic Meters)=             0.633
Gas Volume (Dry Standard Cubic Meters)=      0.662

Barometric Pressure  (mm Hg)=                   767
Static Pressure (mm H20)=                      -434

Percent Oxygen=                                5.7
Percent Carbon Dioxide=                        13.0
Moisture Collected (ml)=                       55.6
Percent Water=                                 10.1

Average Meter Temperature  (C)=                   10
Average Delta H (mm H20)=                      7.3
Average Delta P (mm H20) =                      21.9
Average Stack Temperature  (C)=                   82

Dry Molecular Weight=                        30.31
Wet Molecular Weight=                        29.07

Average Square Root of Delta P  (mm H20)=    4.6772
% Isokinetic=                                100.4

Pitot Coefficient=                             0.84
Sampling Time  (Minutes)=                       80.0
Nozzle Diameter (mm)=                          3.71
Stack Axis #1  (Meters)=                      1.448
Stack Axis #2  (Meters)=                      1.676
Rectangular Stack
Stack Area (Square Meters)=                  2.427

Stack Velocity  (Actual, m/min)=             1,062
Flow rate  (Actual, Cubic m/min)=             2,579
Flow rate  (Standard,  Wet, Cubic m/min)=      2,060
Flow rate  (Standard,  Dry, Cubic m/min)=      1,852

Particulate Loading - Front Half

Particulate Weight (g)=                     0.0222
Particulate Loading,  Dry Std.  (mg/cu m)=       33.5
Particulate Loading,  Actual  (mg/cu m)=         24.1
Emission Rate  (kg/hr)=                         3.72

No Back Half Analysis
                          PROG.=VER  06/27/89
                          11-23-1999  09:15:26
                           Corr.  to  7%  02
                                  30.7
& 12% C02
  31.0
RCA#2 APPENDIX B
                                                53

-------
FILE NAME - 38B
RUN # - 38 - Method 17 Train B  for  PM
LOCATION - Unit 2A Baghouse Outlet  Duct
DATE - 11/19/99 Time: 0137-0257
PROJECT # - 104703.1.002.05.02
'oint #

1
2
3
4
5
6
7
8
9
10
11
12
13
14
15
16
Delta P
(in
0.
0.
0.
0.
0.
0.
0.
0.
0.
0.
0.
0.
0.
0.
0.
0.
. H20)
870
920
900
870
830
790
790
960
920
840
820
820
860
880
870
850
Delta H
(in.
0.
0.
0.
0.
0.
0.
0.
0.
0.
0.
0.
0.
0.
0.
0.
0.
H20)
29
30
30
29
27
26
26
32
31
28
27
27
29
29
29
28
Stack
(F)
178
179
179
179
180
181
180
178
179
181
180
179
180
181
179
179
T Meter T
In(F)
49
48
48
49
49
50
50
51
51
51
51
51
51
52
52
52
Out (F)
48
48
48
49
49
49
49
49
50
50
50
50
50
50
50
51
                                                       PROG.=VER 06/27/89
                                                       11-23-1999  09:15:26
Fraction

DRY CATCH
FILTER

Fraction
                     Final Wt. Tare Wt.  Blank  Wt.  Net Wt
                       (g)        (g)        (g)       (g)
                    0.0000    0.0000     0.0000    0.0000
                    3.3188    3.2989     0.0000    0.0199
                     Final Wt. Tare Wt.    Vol.     Net Wt
                       (g)        (g)       (ml)       (g)
PROBE RINSE         3.6497    3.6474     27.7     0.0023
IMPINGERS           0.0000    0.0000      0.0     0.0000
Probe Rinse Blank  (mg/ml)=  0.0000
Impinger Blank  (mg/ml)=  0.0000
 54
                                 RCA#2 APPENDIX B

-------
FILE NAME - 39A
RUN # - 39 - Method 17 Train A for PM
LOCATION - Unit 2A Baghouse Outlet Duct
DATE - 11/19/99 Time: 0335-0504
PROJECT # - 104703.1.002.05.01

Initial Meter Volume  (Cubic Feet)=         463.012
Final Meter Volume (Cubic Feet)=           484.276
Meter Factor=                                0.996
Final Leak Rate (cu ft/min)=                 0.002
Net Meter Volume  (Cubic Feet)=              21.179
Gas Volume (Dry Standard Cubic Feet)=       22.196

Barometric Pressure  (in Hg) =                 30.20
Static Pressure (Inches H20)=               -16.15

Percent Oxygen=                                5 . 3
Percent Carbon Dioxide=                       13.3
Moisture Collected (ml)=                      54.8
Percent Water=                                10.4

Average Meter Temperature  (F) =                  49
Average Delta H (in H20)=                     0.33
Average Delta P (in H20)=                    1.030
Average Stack Temperature  (F) =                 177

Dry Molecular Weight=                        30.34
Wet Molecular Weight=                        29.05

Average Square Root of Delta P  (in H20)=    0.9415
% Isokinetic=                                100.3
PROG.=VER 06/27/89
11-23-1999  09:15:42
Pitot Coefficient=                            0.84
Sampling Time  (Minutes) =                      75.0
Nozzle Diameter  (Inches) =                    0.146
Stack Axis #1  (Inches) =                       57.0
Stack Axis #2  ( Inches) =                       66.0
Rectangular Stack
Stack Area (Square Feet)=                    26.13

Stack Velocity   (Actual, Feet/min) =          3,525
Flow Rate  (Actual, Cubic ft/min) =           92,098
Flow rate  (Standard, Wet, Cubic f t/min) =    74,051
Flow Rate  (Standard, Dry, Cubic ft/min) =    66,337

Particulate Loading - Front Half

Particulate Weight  (g) =                     0.0311
Particulate Loading, Dry Std.  (gr/scf ) =     0.0216
Particulate Loading, Actual  (gr/cu ft)=     0.0155
Emission Rate  (lb/hr)=                       12.27

No Back Half Analysis
Corr. to 7% 02 & 12% C02
     0.0192    0.0195
                            RCA#2 APPENDIX B
                                                                            55

-------
                        *  * METRIC UNITS  *  *
FILE NAME - 39A
RUN # - 39 - Method 17 Train A for PM
LOCATION - Unit 2A Baghouse Outlet Duct
DATE - 11/19/99 Time: 0335-0504
PROJECT # - 104703.1.002.05.01

Initial Meter Volume  (Cubic Meters)=        13.111
Final Meter Volume  (Cubic  Meters)=          13.713
Meter Factor=                                 0.996
Final Leak Rate  (cu m/min)=                 0.0001
Net Meter Volume  (Cubic Meters)=              0.600
Gas Volume (Dry Standard Cubic Meters)=       0.629

Barometric Pressure  (mm Hg)=                    767
Static Pressure  (mm H20)=                      -410

Percent Oxygen=                                 5.3
Percent Carbon Dioxide=                        13.3
Moisture Collected  (ml)=                       54.8
Percent Water=                                 10.4

Average Meter Temperature  (C)=                   9
Average Delta H  (mm H20)=                       8.4
Average Delta P  (mm H20) =                      26.2
Average Stack Temperature  (C)=                   80

Dry Molecular Weight=                         30.34
Wet Molecular Weight=                         29.05

Average Square Root of Delta P  (mm H20)=    4.7449
% Isokinetic=                                 100.3

Pitot Coefficient=                             0.84
Sampling Time  (Minutes)=                       75.0
Nozzle Diameter  (mm)=                          3.71
Stack Axis #1  (Meters)=                       1.448
Stack Axis #2  (Meters)=                       1.676
Rectangular Stack
Stack Area (Square Meters)=                   2.427

Stack Velocity   (Actual, m/min)=              1,075
Flow rate  (Actual, Cubic m/min)=              2,608
'Flow rate  (Standard, Wet,  Cubic m/min)=       2,097
Flow rate  (Standard, Dry,  Cubic m/min)=       1,878

Particulate Loading - Front Half

Particulate Weight  (g)=                     0.0311
Particulate Loading, Dry Std.  (mg/cu m)=       49.5
Particulate Loading, Actual  (mg/cu m)=        35.6
Emission Rate  (kg/hr)=                         5.57

No Back Half Analysis
PROG.=VER 06/27/89
11-23-1999  09:15:42
Corr. to 7% 02 & 12% C02
       44.1      44.6
 56
                                RCA#2 APPENDIX B

-------
FILE NAME - 39A
RUN # - 39 - Method 17'Train A  for  PM
LOCATION - Unit 2A Baghouse Outlet  Duct
DATE - 11/19/99 Time:  0335-0504
PROJECT # - 104703.1.002.05.01
Point #

 1
 2
 3
 4
 5
 6
 7
 8
 9
 10
 11
 12
 13
 14
 15
 16
 17
 18
 19
 20
 21
 22
 23
 24
 25
                                  PROG.=VER 06/27/89
                                  11-23-1999  09:15:42
Delta P
(in. H20)
1.700
1.700
1.600
0.750
0.200
1.600
1.400
1.300
0.400
0.090
1.500
1.300
1.050
0.450
0.030
1.600
1.000
1.000
0.600
0. 050
1.800
1.800
1.700
1.000
0.120
Delta H
(in.
0.
0.
0.
0.
0.
0.
0.
0.
0.
0.
0.
0.
0.
0.
0.
0.
0.
0.
0.
0.
0.
0.
0.
0.
0.
H20)
55
55
52
24
06
52
45
42
13
02
48
42
34
14
01
52
32
32
19
01
58
58
55
32
03
Stack
(F)
177
177
177
177
176
177
177
177
177
177
177
178
177
177
174
177
179
177
177
172
177
178
177
176
177
T Meter T
In(F)
48
46
48
48
48
48
48
49
50
50
49
49
50
51
51
50
50
51
51
51
50
50
52
52
52
Out (F)
47
47
47
47
47
47
47
47
47
48
48
48
48
48
48
48
48
48
48
48
48
48
49
49
49
Fraction
Final Wt.  Tare Wt. Blank Wt. Net Wt
 (g)         (g)        (g)       (g)
DRY CATCH
FILTER
Fraction

PROBE RINSE
IMPINGERS
Probe Rinse Blank
0.0000
3.3416
Final
(g)
3.5236
0.0000
(mg/ml) =
0.0000
3.3143
Wt . Tare Wt .
(g)
3.5198
0.0000
0.0000
0.0000
0.0000
Vol.
(ml)
21.6
0.0

0.0000
0 .0273
Net Wt
(g)
0.0038
0 .0000

Impinger Blank  (mg/ml)=  0.0000
                            RCA#2 APPENDIX B
                                                                            57

-------
FILE NAME - 39B
RUN # - 39 - Method 17 Train B for PM
LOCATION - Unit 2A Baghouse Outlet Duct
DATE - 11/19/99 Time: 0335-0504
PROJECT # - 104703.1.002.05.02

Initial Meter Volume  (Cubic Feet}=         121.391
Final Meter Volume  (Cubic Feet)=           143.689
Meter Factor=                                1.010
Final Leak Rate (cu ft/min)=                 0.004
Net Meter Volume  (Cubic Feet)=              22.521
Gas Volume (Dry Standard Cubic Feet)=       23.595

Barometric Pressure (in Hg)=                 30.20
Static Pressure (Inches H20)=               -16.15

Percent Oxygen=                                5.3
Percent Carbon Dioxide=                       13.3
Moisture Collected  (ml)=                      57.7
Percent Water=                                10.3

Average Meter Temperature  (F)=                  49
Average Delta H (in H20)=                     0.29
Average Delta P(inH20)=                    0.888
Average Stack Temperature  (F) =                 179

Dry Molecular Weight=                        30.34
Wet Molecular Weight=                        29.07

Average Square Root of Delta P (in H20)=    0.9414
% Isokinetic=                                100.0

Pitot Coefficient=                            0.84
Sampling Time (Minutes)=                      80.0
Nozzle Diameter (Inches)=                    0.146
Stack Axis #1 (Inches)=                       57.0
Stack Axis #2 (Inches)=                       66.0
Rectangular Stack
Stack Area (Square Feet)=                    26.13

Stack Velocity  (Actual, Feet/min)=          3,531
Flow Rate (Actual, Cubic ft/min)=           92,255
Flow rate (Standard, Wet, Cubic ft/min)=    73,881
Flow Rate (Standard, Dry, Cubic ft/min)=    66,250

Particulate Loading - Front Half

Particulate Weight  (g) =                     0.0228
Particulate Loading, Dry Std.  (gr/scf)=     0.0149
Particulate Loading, Actual  (gr/cu ft)=     0.0107
Emission Rate (lb/hr)=                        8.45

No Back Half Analysis
PROG.=VER 06/27/89
11-23-1999  09:15:58
Corr. to 7% 02 & 12% C02
     0.0133    0.0134
 58
                                RCA#2 APPENDIX B

-------
                        * * METRIC UNITS * *
FILE NAME - 39B
RUN # - 39 - Method 17 Train B for PM
LOCATION - Unit 2A Baghouse Outlet Duct
DATE - 11/19/99 Time: 0335-0504
PROJECT # - 104703.1.002.05.02

Initial Meter Volume  (Cubic Meters)=         3.437
Final Meter Volume  (Cubic Meters)=           4.069
Meter Factor=                                1.010
Final Leak Rate (cu m/min)=                 0.0001
Net Meter Volume  (Cubic Meters)=             0.638
Gas Volume  (Dry Standard Cubic Meters)=      0.668

Barometric Pressure  (mm Hg) =                   767
Static Pressure (mm H20)=                     -410

Percent Oxygen=                                5.3
Percent Carbon Dioxide=                       13.3
Moisture Collected  (ml)=                      57.7
Percent Water=                                10.3

Average Meter Temperature  (C)=                   9
Average Delta H (mm H20)=                      7.5
Average Delta P (mm H20)=                     22.5
Average Stack Temperature  (C) =                   82

Dry Molecular Weight=                        30.34
Wet Molecular Weight=                        29.07

Average Square Root of Delta P  (mm H20)=    4.7444
% Isokinetic=                                100.0

Pitot Coefficient=                            0.84
Sampling Time  (Minutes)=                      80.0
Nozzle Diameter (mm)=                         3.71
Stack Axis #1  (Meters)=                      1.448
Stack Axis #2  (Meters)=                      1.676
Rectangular Stack
Stack Area  (Square Meters)=     .             2.427

Stack Velocity  (Actual, m/min)=             1,076
Flow rate  (Actual, Cubic m/min)=             2,612
Flow rate  (Standard, Wet, Cubic m/min)=      2,092
Flow rate  (Standard, Dry, Cubic m/min)=      1,876

Particulate Loading - Front Half

Particulate Weight  (g)=                     0.0228
Particulate Loading, Dry Std.  (mg/cu m)=      34.1
Particulate Loading, Actual  (mg/cu m)=        24.5
Emission Rate  (kg/hr)=                        3.84

No Back Half Analysis
PROG.=VER 06/27/89
11-23-1999  09:15:58
Corr. to 7% 02 & 12% C02
       30.4      30.8
                            RCA#2 APPENDIX B
                                                                            59

-------
FILE NAME - 39B
RUN # - 39 - Method 17 Train B  for  PM
LOCATION - Unit 2A Baghouse Outlet  Duct
DATE - 11/19/99 Time: 0335-0504
PROJECT # - 104703.1.002.05.02
Point #

 1
 2
 3
 4
 5
 6
 7
 8
 9
 10
 11
 12
 13
 14
 15
 16
                                   PROG.=VER 06/27/89
                                   11-23-1999  09:15:58
Delta P
in
0.
0.
0.
0.
0.
0.
0.
0.
0.
0.
0.
0.
0.
1.
0.
0.
. H20)
900
880
870
920
840
840
760
970
920
860
840
800
920
050
970
860
Delta H
(in.
0.
0.
0.
0.
0.
0.
0.
0.
0.
0.
0.
0.
0.
0.
0.
0.
H20)
30
29
29
30
28
28
25
32
31
28
28
26
31
35
32
29
Stack
(F)
179
179
179
180
179
179
180
180
179
180
180
179
179
180
179
178
T Meter T
In(F)
48
48
48
48
49
49
49
49
49
49
50
49
49
50
50
50
Out (F)
48
48
48
48
48
48
49
49
49
49
49
49
49
49
49
50
Fraction

DRY CATCH
FILTER

Fraction
 Final Wt.  Tare Wt.  Blank Wt. Net Wt,
  (g)        (g)        (g)       (g)
0.0000    0.0000    0.0000    0.0000
3.3137    3.2929    0.0000    0.0208
 Final Wt.  Tare Wt.
  (g)        (g)
PROBE RINSE         3.7299     3.7279
IMPINGERS           0.0000     0.0000
Probe Rinse Blank  (mg/ml)=   0.0000
Impinger Blank  (mg/ml)=   0.0000
  Vol.
 (ml)
23.4
 0.0
  Net Wt,
   (g)
0.0020
0.0000
 60
                                 RCA#2 APPENDIX B

-------
FILE NAME - 40A
RUN # - 40 - Method 17 Train A for PM
LOCATION - Unit 2A Baghouse Outlet Duct
DATE - 11/20/99 Time: 0900-1020
PROJECT # - 104703.1.002.05.01

Initial Meter Volume  (Cubic Feet)=         485.988
Final Meter Volume  (Cubic Feet)=           507.367
Meter Factor=                                0.996
Final Leak Rate (cu ft/min)=                 0.004
Net Meter Volume  (Cubic Feet)=              21.293
Gas Volume (Dry Standard Cubic Feet)=       21.591

Barometric Pressure  (in Hg)=                 30.08
Static Pressure (Inches H20)=               -17.10

Percent Oxygen=                                6.3
Percent Carbon Dioxide=                       12.5
Moisture Collected  (ml)=                      64.7
Percent Water=                                12.4

Average Meter Temperature  (F)=                   64
Average Delta H (in H20)=                     0.32
Average Delta P (in H20)=                    1.033
Average Stack Temperature  (F)=                 179

Dry Molecular Weight=                        30.25
Wet Molecular Weight=                        28.74

Average Square Root of Delta P  (in H20)=    0.9439
% Isokinetic=                                 99.4

Pitot Coefficient=                            0.84
Sampling Time  (Minutes)=                      75.0
Nozzle Diameter (Inches)=                    0.146
Stack Axis #1  (Inches)=                       57.0
Stack Axis #2  (Inches)=                       66.0
Rectangular Stack
Stack Area (Square Feet)=                    26.13

Stack Velocity  (Actual, Feet/min)=          3,572
Flow Rate  (Actual, Cubic ft/min)=           93,323
Flow rate  (Standard, Wet, Cubic ft/min)=    74,270
Flow Rate  (Standard, Dry, Cubic ft/min)=    65,084

Particulate Loading - Front Half

Particulate Weight  (g)=                     0.0107
Particulate Loading, Dry Std.  (gr/scf)=     0.0076
Particulate Loading, Actual  (gr/cu ft)=     0.0053
Emission Rate  (lb/hr)=                        4.26

No Back Half Analysis
PROG.=VER 06/27/89
11-23-1999  09:16:08
Corr. to 7% 02 & 12% C02
     0.0073    0.0073
                            RCA#2 APPENDIX B
                                                                            61

-------
                        *  * METRIC UNITS  *  *
FILE NAME - 40A
RUN # - 40 - Method 17 Train A for PM
LOCATION - Unit 2A Baghouse Outlet Duct
DATE - 11/20/99 Time: 0900-1020
PROJECT # - 104703.1.002.05.01

Initial Meter Volume  (Cubic Meters)=        13.761
Final Meter Volume  (Cubic  Meters)=          14.367
Meter Factor=                                 0.996
Final Leak Rate  (cu m/min)=                 0.0001
Net Meter Volume  (Cubic Meters)=              0.603
Gas Volume (Dry Standard Cubic Meters)=       0.611

Barometric Pressure  (mm Hg)=                    764
Static Pressure  (mm H20)=                      -434

Percent Oxygen=                                 6.3
Percent Carbon Dioxide=                        12.5
Moisture Collected  (ml)=                       64.7
Percent Water=                                 12.4

Average Meter Temperature  (C)=                   18
Average Delta H  (mm H20)=                       8.1
Average Delta P  (mm H20)=                      26.2
Average Stack Temperature  (C)=                   82

Dry Molecular Weight=                         30.25
Wet Molecular Weight=                         28.74

Average Square Root of Delta P  (mm H20) =    4.7571
% Isokinetic=                                  99.4

Pitot Coefficient^                             0.84
Sampling Time  (Minutes)=                       75.0
Nozzle Diameter  (mm)=                          3.71
Stack Axis #1  (Meters)=                       1.448
Stack Axis #2  (Meters)=                       1.676
Rectangular Stack
Stack Area (Square Meters)=                   2.427

Stack Velocity   (Actual, m/min)=              1,089
Flow rate (Actual, Cubic m/min)=              2,643
'Flow rate (Standard, Wet,  Cubic m/min)=       2,103
Flow rate (Standard, Dry,  Cubic m/min)=       1,843

Particulate Loading - Front Half

Particulate Weight  (g)=                     0.0107
Particulate Loading, Dry Std.  (mg/cu m)=       17.5
Particulate Loading, Actual  (mg/cu m)=        12.2
Emission Rate  (kg/hr)=                         1.93

No Back Half Analysis
PROG.=VER 06/27/89
11-23-1999  09:16:08
Corr. to 7% 02
       16.7
12% C02
16.8
 62
                                RCA#2 APPENDIX B

-------
FILE NAME - 40A
RUN # - 40 - Method 17 Train A  for PM
LOCATION - Unit 2A Baghouse Outlet Duct
DATE - 11/20/99 Time: 0900-1020
PROJECT # - 104703.1.002.05.01
Point #

 1
 2
 3
 4
 5
 6
 7
 8
 9
 10
 11
 12
 13
 14
 15
 16
 17
 18
 19
 20
 21
 22
 23
 24
 25
                                                       PROG.=VER  06/27/89
                                                       11-23-1999  09:16:09
Delta P
in. H20)
1.700
1.700
1.500
0. 770
0.110
1.500
1.400
1.100
0.460
0.060
1.300
1.100
0.970
0.400
0.040
1.600
1.600
1.400
0.570
0. 080
1.800
1.800
1.400
1.300
0.170
Delta H
(in. H20)
0.53
0.52
0.46
0.24
0.03
0.46
0.43
0.34
0.14
0.01
0.40
0.34
0.30
0.12
0.01
0.50
0.50
0.44
0.18
0.02
0.57
0.57
0.44
0.41
0.05
Stack
•(F)
179
181
179
177
174
179
180
179
178
177
179
179
178
178
178
179
180
180
179
178
179
182
182
183
181
T Meter T
In(F)
57
58
59
59
61
60
61
63
64
63
63
65
66
66
67
66
67
69
70
70
70
70
72
74
74
Out (F)
57
57
58
58
58
58
59
60
60
60
61
61
62
62
63
63
64
65
65
65
66
67
67
68
68
Fraction

DRY CATCH
FILTER

Fraction
                     Final Wt. Tare Wt. Blank Wt. Net  Wt,
                       (g)        (g)        (g)       (g)
                    0.0000    0.0000    0.0000    0.0000
                    3.3183    3.3086    0.0000    0.0097
                     Final Wt
                       (g)
PROBE RINSE         3 .5353
IMPINGERS           0.0000
Probe Rinse Blank  (mg/ml)=
   Tare Wt.
    (g)
  3.5343
  0.0000
0.0000
  Vol.
 (ml)
19.5
 0.0
  Net Wt
   (g)
0.0010
0.0000
Impinger Blank  (mg/ml)=   0.0000
                            RCA#2 APPENDIX B
                                                                             63

-------
FILE NAME - 4OB
RUN # - 40 - Method  17 Train B  for PM
LOCATION - Unit 2A Baghouse Outlet Duct
DATE - 11/20/99 Time: 0900-1020
PROJECT # - 104703.1.002.05.02

Initial Meter Volume  (Cubic Feet)=          153.440
Final Meter Volume  (Cubic Feet)=            174.366
Meter Factor=                                 1.010
Final Leak Rate  (cu  ft/min)=                  0.002
Net Meter Volume  (Cubic Feet)=               21.135
Gas Volume (Dry Standard Cubic  Feet)=        21.430

Barometric Pressure  (in Hg)=                  30.08
Static Pressure  (Inches H20)=                -17.10

Percent Oxygen=                                 6.3
Percent Carbon Dioxide=                        12.5
Moisture Collected  (ml}=                       64.3
Percent Water=                                 12.4

Average Meter Temperature  (F}=                   64
Average Delta H  (in H20}=                      0.25
Average Delta P  (in H20)=                     0.779
Average Stack Temperature  (F)=                  181

Dry Molecular Weight=                         30.25
Wet Molecular Weight=                         28.73

Average Square Root of Delta P  (inH20)=     0.8808
% Isokinetic=                                  99.3

Pitot Coefficient=                             0.84
Sampling Time (Minutes)=                       80.0
Nozzle Diameter  (Inches)=                     0.146
Stack Axis #1 (Inches)=                        57.0
Stack Axis #2 (Inches)=                        66.0
Rectangular Stack
Stack Area (Square Feet)=                     26.13

Stack Velocity   (Actual, Feet/min)=           3,339
Flow Rate (Actual, Cubic ft/min)=            87,237
Flow rate (Standard, Wet, Cubic ft/min)=     69,182
'Flow Rate (Standard, Dry, Cubic f t/min) =     60,616

Particulate Loading  - Front Half

Particulate Weight  (g)=                      0.0089
Particulate Loading, Dry Std.  (gr/scf)=      0.0064
Particulate Loading, Actual  (gr/cu ft)=      0.0044
Emission Rate (lb/hr)=                         3.32

No Back Half Analysis
PROG.=VER 06/27/89
11-23-1999  09:16:19
Corr. to 7% 02 & 12% C02
     0.0061    0.0061
 64
                                RCA#2 APPENDIX B

-------
                        * * METRIC UNITS * *
FILE NAME - 4 OB
RUN # - 40 - Method 17 Train B for PM
LOCATION - Unit 2A Baghouse Outlet Duct
DATE - 11/20/99 Time: 0900-1020
PROJECT # - 104703.1.002.05.02

Initial Meter Volume  (Cubic Meters)=         4.345
Final Meter Volume (Cubic Meters)=           4.937
Meter Factor=                                1.010
Final Leak Rate (cu m/min)=                 0.0001
Net Meter Volume  (Cubic Meters)=             0.598
Gas Volume (Dry Standard Cubic Meters)=      0.607

Barometric Pressure  (mm Hg)=                   764
Static Pressure (mm H20) =                     -434

Percent Oxygen=                                6.3
Percent Carbon Dioxide=                       12.5
Moisture Collected (ml)=                      64.3
Percent Water=                                12.4

Average Meter Temperature  (C)=                   18
Average Delta H (mm H20)=                      6.3
Average Delta P (mm H20) =                     19.8
Average Stack Temperature  (C)=                   83

Dry Molecular Weight=                        30.25
Wet Molecular Weight=                        28.73

Average Square Root of Delta P  (mm H20)=    4.4390
% Isokinetic=                                 99.3

Pitot Coefficient=                            0.84
Sampling Time  (Minutes)=                      80.0
Nozzle Diameter (mm)=                         3.71
Stack Axis #1  (Meters)=                      1.448
Stack Axis #2  (Meters)=                      1.676
Rectangular Stack
Stack Area (Square Meters)=                  2.427

Stack Velocity  (Actual, m/min)=             1,018
Flow rate  (Actual, Cubic m/min)=             2,470
Flow rate  (Standard,  Wet, Cubic m/min)=      1,959
Flow rate  (Standard,  Dry, Cubic m/min)=      1,716

Particulate Loading  - Front Half

Particulate Weight (g)=                     0.0089
Particulate Loading,  Dry Std.  (mg/cu m)=      14.7
Particulate Loading,  Actual  (mg/cu m)=        10.2
Emission Rate  (kg/hr)=                        1.51

No Back Half Analysis
PROG.=VER 06/27/89
11-23-1999  09:16:19
Corr. to 7% 02 & 12% C02
       14.0      14.1
                            RCA#2 APPENDIX B
                                                                            65

-------
FILE NAME - 4OB
RUN # - 40 - Method 17 Train B  for PM
LOCATION - Unit 2A Baghouse Outlet Duct
DATE - 11/20/99 Time: 0900-1020
PROJECT # - 104703.1.002.05.02
Point #

 1
 2
 3
 4
 5
 6
 7
 8
 9
 10
 11
 12
 13
 14
 15
 16
                                  PROG.=VER  06/27/89
                                  11-23-1999   09:16:19
Delta P
(in
0.
0.
0.
0.
0.
0.
0.
0.
0.
0.
0.
0.
0.
0.
1.
0.
. H20)
780
800
820
700
700
730
650
670
720
700
750
770
820
790
100
970
Delta H
(in.
0.
0.
0.
0.
0.
0.
0.
0.
0.
0.
0.
0.
0.
0.
0.
0.
H20)
25
25
26
22
22
23
21
21
23
22
24
25
26
25
36
31
Stack
(F)
181
182
179
180
182
180
181
182
180
181
182
182
181
182
184
183
T Meter T
In(F)
59
59
60
60
61
62
63
64
65
66
66
68
68
70
71
72
Out (F)
58
58
59
59
59
60
61
62
63
64
64
65
66
67
68
69
Fraction

DRY CATCH
FILTER

Fraction
PROBE RINSE         3.5574
IMPINGERS           0.0000
Probe Rinse Blank  (mg/ml)=
Impinger Blank  (mg/ml)=  0.0000
 Final Wt. Tare Wt.  Blank Wt. Net Wt
  (g)         (g)        (g)       (g)
o.oooo    o.oooo    o.oooo    o.oooo
3.3225    3.3157    0.0000    0.0068
                       (g)
t. Tare Wt.
(g)
3.5553
0.0000
0.0000
Vol.
(ml)
33 .2
0.0

Net Wt
(g)
0.0021
0.0000

 66
                                RCA#2 APPENDIX B

-------
FILE NAME - 41A
RUN # - 41 - Method 17 Train A for PM
LOCATION - Unit 2A Baghouse Outlet Duct
DATE - 11/20/99 Time: 1112-1231
PROJECT # - 104703.1.002.05.01

Initial Meter Volume  (Cubic Feet)=          507.643
Final Meter Volume  (Cubic Feet)=            530.756
Meter Factor=                                 0.996
Final Leak Rate  (cu ft/min)=                  0.001
Net Meter Volume  (Cubic Feet)=              23.021
Gas Volume (Dry Standard Cubic Feet)=       22.684

Barometric Pressure  (in Hg)=                  30.07
Static Pressure  (Inches H20)=               -18.10

Percent Oxygen=                                 5 . 9
Percent Carbon Dioxide=                       13.3
Moisture Collected  (ml)=                      68.4
Percent Water=                                12.4

Average Meter Temperature  (F)=                   79
Average Delta H  (in H20)=                     0.37
Average Delta P  (in H20)=                     1.152
Average Stack Temperature  (F)=                  180

Dry Molecular Weight=                         30.36
Wet Molecular Weight=                         28.83

Average Square Root of Delta P (in H20)=    0.9915
% Isokinetic=                                 99.9

Pitot Coefficient=                            0.84
Sampling Time  (Minutes)=                      75.0
Nozzle Diameter  (Inches)=                     0.146
Stack Axis #1  (Inches)=                       57.0
Stack Axis #2  (Inches)=                       66.0
Rectangular Stack
Stack Area (Square Feet)=                     26.13

Stack Velocity   (Actual, Feet/min)=           3,754
Flow Rate (Actual, Cubic ft/min)=           98,076
Flow rate (Standard, Wet, Cubic ft/min)=    77,729
Flow Rate (Standard, Dry, Cubic ft/min)=    68,063

Particulate Loading - Front Half

Particulate Weight  (g)=                     0.0223
Particulate Loading, Dry Std. (gr/scf)=     0.0151
Particulate Loading, Actual  (gr/cu ft)=     0.0105
Emission Rate  (lb/hr)=                        8.83

No Back Half Analysis
                           PROG.=VER 06/27/89
                           11-23-1999  09:16:31
                           Corr.  to 7% 02 & 12% C02
                                0.0140    0.0137
RCA#2 APPENDIX B
                                                67

-------
                        * * METRIC UNITS * *
FILE NAME - 41A
RUN # - 41 - Method 17 Train A for PM
LOCATION - Unit 2A Baghouse Outlet Duct
DATE - 11/20/99 Time: 1112-1231
PROJECT # - 104703.1.002.05.01

Initial Meter Volume  (Cubic Meters)=        14.374
Final Meter Volume (Cubic Meters)=          15.029
Meter Factor=                                0.996
Final Leak Rate (cu m/min)=                 0.0000
Net Meter Volume  (Cubic Meters)=             0.652
Gas Volume (Dry Standard Cubic Meters)=      0.642

Barometric Pressure  (mm Hg)=                   764
Static Pressure (mm H20)=                     -460

Percent Oxygen=                                5 . 9
Percent Carbon Dioxide=                       13.3
Moisture Collected (ml)=                      68.4
Percent Water=                                12.4

Average Meter Temperature (C)=              ,    26
Average Delta H (mm H20)=                      9.4
Average Delta P (mm H20)=                     29.3
Average Stack Temperature (C)=                  82

Dry Molecular Weight=                        30.36
Wet Molecular Weight=                        28.83

Average Square Root of Delta P (mm H20)=    4.9969
% Isokinetic=                                 99.9

Pitot Coefficient=                            0.84
Sampling Time (Minutes)=                      75.0
Nozzle Diameter (mm)=                         3.71
Stack Axis #1 (Meters)=                      1.448
Stack Axis #2 (Meters)=                      1.676
Rectangular Stack
Stack Area (Square Meters)=                  2.427

Stack Velocity  (Actual, m/min)=             1,144
Flow rate (Actual, Cubic m/min)=             2,777
Flow rate (Standard,  Wet, Cubic m/min)=      2,201
Flow rate (Standard,  Dry, Cubic m/min)=      1,927

Particulate Loading - Front Half

Particulate Weight (g)=                     0.0223
Particulate Loading,  Dry Std.  (mg/cu m) =      34.7
Particulate Loading,  Actual  (mg/cu m)=        24.1
Emission Rate (kg/hr)=                        4.01

No Back Half Analysis
PROG.=VER 06/27/89
11-23-1999  09:16:31
Corr. to 7% 02 & 12% C02
       32.2      31.3
 68
                                RCA#2 APPENDIX B

-------
FILE NAME - 41A
RUN # - 41 - Method 17 Train A  for PM
LOCATION - Unit 2A Baghouse Outlet Duct
DATE - 11/20/99 Time: 1112-1231
PROJECT # - 104703.1.002.05.01
Point #

 1
 2
 3
 4
 5
 6
 7
 8
 9
 10
 11
 12
 13
 14
 15
 16
 17
 18
 19
 20
 21
 22
 23
 24
 25
                                   PROG.=VER 06/27/89
                                   11-23-1999  09:16:31
Delta P
in. H20)
1.700
1.700
1.600
0.780
0.120
1.700
1.600
1.300
0.570
0.050
1.700
1.400
1.400
0.500
0.030
1.700
1.700
1.500
0.530
0.030
1.900
2.100
1.500
1.500
0.190
Delta H
(in
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
. H20)
.54
.54
.51
.25
.03
.54
.51
.42
.18
.01
.54
.45
.45
.16
.01
.55
.55
.48
.17
.01
.62
.68
.48
.49
.06
Stack
(F)
180
181
182
181
180
181
181
180
182
180
182
180
180
179
179
180
179
179
181
176
179
180
180
177
179
T Meter T
In(F)
74
75
76
77
77
77
77
79
80
80
79
80
81
82
82
81
82
83
83
84
82
83
84
85
86
Out (F)
74
74
74
74
75
75
75
76
76
76
76
77
77
78
78
78
79
79
79
79
80
80
80
80
81
Fraction

DRY CATCH
FILTER

Fraction
 Final Wt.  Tare Wt. Blank Wt. Net Wt,
  (g)        (g)        (g)       (g)
o.oooo    o.oooo    o.oooo    o.oooo
3.3323    3.3124    0.0000    0.0199
PROBE RINSE
IMPINGERS
Probe Rinse Blank  (mg/ml)=
 Final Wt.  Tare Wt.    Vol.    Net Wt,
  (g)        (g)       (ml)       (g)
3.3624    3.3600    29.9    0.0024
0.0000    0.0000      0.0    0.0000
        0.0000
Impinger Blank  (mg/ml)=  0.0000
                            RCA#2 APPENDIX B
                                                                            69

-------
FILE NAME - 4IB
RUN # - 41 - Method 17 Train B for PM
LOCATION - Unit 2A Baghouse Outlet Duct
DATE - 11/20/99 Time: 1112-1232
PROJECT # - 104703.1.002.05.02

Initial Meter Volume  (Cubic Feet)=         174.154
Final Meter Volume  (Cubic Feet) =           198.331
Meter Factor=                                1.010
Final Leak Rate (cu ft/min)=                 0.002
Net Meter Volume  (Cubic Feet)=              24.419
Gas Volume (Dry Standard Cubic Feet)=       24.054

Barometric Pressure  (in Hg)=                 30.07
Static Pressure (Inches H20)=               -18.10

Percent Oxygen=                                5 . 9
Percent Carbon Dioxide=                       13.3
Moisture Collected  (ml) =                      72.2
Percent Water=                                12.4

Average Meter Temperature  (F)=                   79
Average Delta H (in H20)=                     0.33
Average Delta P (in H20)=                    0.991
Average Stack Temperature  (F)=                 182

Dry Molecular Weight=                        30.36
Wet Molecular Weight=                        28.83

Average Square Root of Delta P (in H20)=    0.9912
% Isokinetic=                                 99.4

Pitot Coefficient=                            0.84
Sampling Time (Minutes)=                      80.0
Nozzle Diameter (Inches)=                    0.146
Stack Axis #1 (Inches)=                       57.0
Stack Axis #2 (Inches)=                       66.0
Rectangular Stack
Stack Area (Square Feet)=                    26.13

Stack Velocity  (Actual, Feet/min)=          3,759
Flow Rate (Actual, Cubic ft/min)=           98,212
.Flow rate (Standard, Wet, Cubic f t/min) =    77,562
Flow Rate (Standard, Dry, Cubic ft/min)=    67,955

Particulate Loading - Front Half

Particulate Weight  (g)=                     0.0136
Particulate Loading, Dry Std.  (gr/scf)=     0.0087
Particulate Loading, Actual  (gr/cu ft)=     0.0060
Emission Rate (Ib/hr)=                        5.07

No Back Half Analysis
PROG.=VER 06/27/89
11-23-1999  09:16:42
Corr. to 7% 02 & 12% C02
     0.0081    0.0079
 70
                                RCA#2 APPENDIX B

-------
                        * * METRIC UNITS * *
FILE NAME - 4IB
RUN # - 41 - Method 17 Train B for PM
LOCATION - Unit 2A Baghouse Outlet Duct
DATE - 11/20/99 Time: 1112-1232
PROJECT # - 104703.1.002.05.02

Initial Meter Volume  (Cubic Meters)=         4.931
Final Meter Volume  (Cubic Meters)=           5.616
Meter Factor=                                1.010
Final Leak Rate (cu tn/min) =                 0.0001
Net Meter Volume  (Cubic Meters)=             0.691
Gas Volume (Dry Standard Cubic Meters)=      0.681

Barometric Pressure  (mm Hg)=                   764
Static Pressure (mm H20)=                     -460
PROG.=VER 06/27/89
11-23-1999  09:16:42
Percent Oxygen=                                5 . 9
Percent Carbon Dioxide=                       13.3
Moisture Collected  (ml)=                      72.2
Percent Water=                                12.4

Average Meter Temperature  (C)=                   26
Average Delta H  (mm H20)=                      8.3
Average Delta P  (mm H20) =                     25.2
Average Stack Temperature  (C)=                   83

Dry Molecular Weight=                        30.36
Wet Molecular Weight=                        28.83

Average Square Root of Delta P  (mm H20)=    4.9955
% Isokinetic=                                 99.4

Pitot Coefficient=                            0.84
Sampling Time (Minutes)=                      80.0
Nozzle Diameter  (mm)=                         3.71
Stack Axis #1 (Meters)=                      1.448
Stack Axis #2 (Meters)=                      1.676
Rectangular Stack
Stack Area (Square Meters)=                  2.427

Stack Velocity   (Actual, m/min)=             1,146
Flow rate  (Actual, Cubic m/min)=             2,781
Flow rate  (Standard, Wet, Cubic m/min)=      2,196
Flow rate  (Standard, Dry, Cubic m/min)=      1,924

Particulate Loading - Front Half

Particulate Weight  (g)=                     0.0136
Particulate Loading, Dry Std.  (mg/cu m)=      20.0
Particulate Loading, Actual  (mg/cu m)=        13.8
Emission Rate (kg/hr)=                        2.30

No Back Half Analysis
Corr. to 7% 02 & 12% C02
       18.5      18.0
                            RCA#2 APPENDIX B
                                                                            71

-------
FILE NAME - 4IB
RUN # - 41 - Method 17 Train B  for  PM
LOCATION - Unit 2A Baghouse Outlet  Duct
DATE - 11/20/99 Time: 1112-1232
PROJECT # - 104703.1.002.05.02
Point #

 1
 2
 3
 4
 5
 6
 7
 8
 9
 10
 11
 12
 13
 14
 15
 16
                                  PROG.=VER  06/27/89
                                  11-23-1999   09:16:42
Delta P
in
0.
0.
1.
0.
0.
0.
1.
0.
1.
1.
1.
0.
1.
0.
1.
1.
. H20)
840
630
000
930
890
910
000
880
000
100
000
940
000
930
400
400
Delta H
(in.
0.
0.
0.
0.
0.
0.
0.
0.
0.
0.
0.
0.
0.
0.
0.
0.
H20)
27
20
33
30
29
30
33
29
33
36
33
31
33
31
47
47
Stack
(F)
182
183
183
183
183
183
184
183
182
181
181
182
181
182
182
180
T Meter T
In(F)
74
75
75
76
78
78
79
80
81
81
82
83
83
83
84
84
Out (F)
73
74
74
75
76
76
77
78
79
79
80
81
81
82
82
82
Fraction

DRY CATCH
FILTER

Fraction
 Final Wt. Tare Wt.  Blank Wt. Net Wt
  (g)        (g)        (g)       (g)
0.0000    0.0000    0.0000    0.0000
3.3070    3.2939    0.0000    0.0131
 Final Wt.  Tare Wt.
  (g)        (g)
PROBE RINSE         3.3260    3.3255
IMPINGERS           0.0000    0.0000
Probe Rinse Blank  (mg/ml)=   0.0000
Impinger Blank  (mg/ml)=  0.0000
  Vol.
 (ml)
32.2
 0.0
  Net Wt
   (g)
0.0005
0.0000
 72
                                RCA#2 APPENDIX B

-------
 FILE NAME  -  42A
 RUN #  - 42  - Method  17  Train A for PM
 LOCATION - Unit 2A Baghouse  Outlet Duct
 DATE - 11/20/99 Time: 1350-1512
 PROJECT #  -  104703.1.002.05.01

 Initial Meter Volume (Cubic  Feet)=         531.164
 Final Meter  Volume (Cubic  Feet)=            553.900
 Meter Factor=                                 0.996
 Final Leak Rate (cu  ft/min)=                 0.003
 Net Meter Volume (Cubic Feet)=              22.645
 Gas Volume  (Dry Standard Cubic Feet)=       22.059

 Barometric Pressure  (in Hg)=                 29.98
 Static Pressure (Inches H20)=               -18.07

 Percent Oxygen=                                5.1
 Percent Carbon  Dioxide=                       14.1
 Moisture Collected (ml)=                      66.0
 Percent Water=                                 12.4

 Average Meter Temperature  (F)=                  83
 Average Delta H (in  H20)=                      0.35
 Average Delta P (in  H20)=                     1.092
 Average Stack Temperature  (F)=                 181

 Dry Molecular Weight=                         30.46
 Wet Molecular Weight=                         28.92

 Average Square  Root  of  Delta P (in H20)=     0.9699
 %  Isokinetic=                                  99.6

 Pitot Coefficient=                            0.84
 Sampling Time  (Minutes)=                      75.0
 Nozzle Diameter (Inches)=                     0.146
 Stack Axis #1  (Inches)=                       57.0
 Stack Axis #2  (Inches)=                       66.0
 Rectangular  Stack
 Stack Area  (Square Feet)=                     26.13

 Stack Velocity   (Actual, Feet/min)=          3,675
 Flow Rate  (Actual, Cubic ft/min)=            96,004
 Flow rate  (Standard, Wet,  Cubic ft/min)=     75,745
 Flow Rate  (Standard, Dry,  Cubic ft/min)=     66,390

•Particulate  Loading  - Front  Half

 Particulate  Weight (g)=                     0.0346
 Particulate  Loading, Dry Std.  (gr/scf)=      0.0242
 Particulate  Loading, Actual  (gr/cu ft)=      0.0167
 Emission Rate  (lb/hr)=                        13.74

 No Back Half Analysis
                           PROG.=VER  06/27/89
                           11-23-1999  09:16:53
                           Corr.  to  7%  02  & 12% C02
                                0.0213     0.0206
RCA#2 APPENDIX B
                                                73

-------
                         *  * METRIC UNITS  *  *
FILE NAME - 42A
RUN # - 42 - Method 17 Train A for PM
LOCATION - Unit 2A Baghouse Outlet Duct
DATE - 11/20/99 Time: 1350-1512
PROJECT # - 104703.1.002.05.01

Initial Meter Volume  (Cubic Meters)=        15.040
Final Meter Volume  (Cubic  Meters)=          15.684
Meter Factor=                                 0.996
Final Leak Rate (cu m/min)=                 0.0001
Net Meter Volume  (Cubic  Meters)=              0.641
Gas Volume (Dry Standard Cubic Meters)=       0.625

Barometric Pressure (mm  Hg)=                    761
Static Pressure (mm H20)=                      -459

Percent Oxygen=                                 5.1
Percent Carbon Dioxide=                        14.l
Moisture Collected  (ml)=                      66.0
Percent Water=                                 12.4

Average Meter Temperature  (C}=                  29
Average Delta H (mm H20)=                       8.9
Average Delta P (mm H20)=                      27.7
Average Stack Temperature  (C) =                  83

Dry Molecular Weight=                         30.46
Wet Molecular Weight=                         28.92

Average Square Root of Delta P (mm H20)=    4.8883
% Isokinetic=                                  99.6

Pitot Coefficient=                             0.84
Sampling Time (Minutes)=                      75.0
Nozzle Diameter (mm)=                          3.71
Stack Axis #1 (Meters)=                       1.448
Stack Axis #2 (Meters)=                       1.676
Rectangular Stack
Stack Area (Square Meters)=                   2.427

Stack Velocity  (Actual, m/min)=              1,120
Flow rate (Actual, Cubic m/min)=              2,719
Flow rate (Standard, Wet,  Cubic m/min)=       2,145
Flow rate (Standard, Dry,  Cubic m/min)=       1,880

Particulate Loading - Front Half

Particulate Weight  (g)=                     0.0346
Particulate Loading, Dry Std.  (mg/cu m)=       55.4
Particulate Loading, Actual  (mg/cu m)=         38.3
Emission Rate (kg/hr)=                         6.24

No Back Half Analysis
PROG.=VER 06/27/89
11-23-1999  09:16:53
Corr. to 7% 02 & 12% C02
       48.8      47.1
 74
                                RCA#2 APPENDIX B

-------
FILE NAME - 42A
RUN # - 42 - Method 17 Train A for PM
LOCATION - Unit 2A Baghouse Outlet Duct
DATE - 11/20/99 Time: 1350-1512
PROJECT # - 104703.1.002.05.01
Point #

 1
 2
 3
 4
 5
 6
 7
 8
 9
 10
 11
 12
 13
 14
 15
 16
 17
 18
 19
 20
 21
 22
 23
 24
 25
                                  PROG.=VER 06/27/89
                                  11-23-1999  09:16:53
Delta P
in. H20)
1.600
1.600
1.500
0.700
0.270
1.800
1.800
1.500
0.630
0.060
1.700
1.500
1.200
0.350
0.030
1.700
1.700
1. 050
0.620
0.030
1.700
1.700
1.100
1.300
0.170
Delta H
(in. H20)
0.51
0.51
0.48
0.22
0.08
0.58
0.58
0.48
0.20
0.01
0.55
0.48
0.39
0.11
0.01
0.55
0.55
0.34
0.20
0.01
0.55
0.55
0.35
0.42
0.05
Stack
(F)
182
182
183
182
182
180
182
181
181
179
179
182
182
180
178
181
181
181
182
176
180
180
183
181
181
T Meter T
In(F)
80
80
81
81
82
82
82
84
84
85
84
85
• 86
86
86
85
85
87
88
86
85
86
86
87
88
Out (F)
80
80
80
80
80
80
81
81
81
81
82
82
82
82
83
83
83
84
84
85
84
85
84
85
85
Fraction

DRY CATCH
FILTER

Fraction

PROBE RINSE
IMPINGERS
 Final Wt. Tare Wt.  Blank Wt.  Net Wt
  (g)        (g)        (g)       (g)
0.0000    0.0000    0.0000    0.0000
3.3485    3.3191    0.0000    0.0294
 Final Wt.
  (g)
3.7267
0. 0000
 Tare Wt.    Vol.
Probe Rinse Blank  (mg/ml)=   0
Impinger Blank  (mg/ml)=   0.0000
  (g)
3.7215
0.0000
0000
 (ml]
30.1
 0.0
  Net Wt
   (g)
0.0052
0.0000
                            RCA#2 APPENDIX B
                                                                             75

-------
FILE NAME  - 42B
RUN # - 42 - Method  17 Train  B  for  PM
LOCATION - Unit  2A Baghouse Outlet  Duct
DATE - 11/20/99  Time: 1350-1512
PROJECT #  - 104703.1.002.05.02

Initial Meter Volume  (Cubic Feet)=          208.689
Final Meter Volume  (Cubic  Feet)=            231.754
Meter Factor=                                 1.010
Final Leak Rate  (cu  ft/min)=                  0.001
Net Meter Volume  (Cubic Feet)=               23.296
Gas Volume (Dry  Standard Cubic  Feet)=        22.643

Barometric Pressure  (in Hg)=                  29.98
Static Pressure  (Inches H20)=                -18.07

Percent Oxygen=                                 5.i
Percent Carbon Dioxide=                       14.1
Moisture Collected  (ml)=                      60.9
Percent Water=                                11.2

Average Meter Temperature  (F)=                   84
Average Delta H  (in H20)=                     0.29
Average Delta P  (in H20)=                     0.875
Average Stack Temperature  (F)=                  184

Dry Molecular Weight=                         30.46
Wet Molecular Weight=                         29.06

Average Square Root of Delta  P  (in  H20)=     0.9323
% Isokinetic=                                 98.9

Pitot Coefficient=                            0.84
Sampling Time (Minutes)=                      80.0
Nozzle Diameter  (Inches)=                     0.146
Stack Axis #1 (Inches)=                       57.0
Stack Axis #2 (Inches)=                       66.0
Rectangular Stack
Stack Area (Square Feet)=                     26.13

Stack Velocity   (Actual, Feet/min)=           3,532
Flow Rate  (Actual, Cubic ft/min)=            92,262
•Flow rate  (Standard, Wet,  Cubic f t/min) =     72,471
Flow Rate  (Standard, Dry,  Cubic ft/min)=     64,323

Particulate Loading  - Front Half

Particulate Weight  (g)=                      0.0210
Particulate Loading, Dry Std.  (gr/scf)=      0.0143
Particulate Loading, Actual  (gr/cu  ft)=      0.0100
Emission Rate (lb/hr)=                        7.87

No Back Half Analysis
PROG.=VER 06/27/89
11-23-1999  09:17:04
Corr. to 7% 02 & 12% C02
     0.0126    0.0122
 76
                                RCA#2 APPENDIX B

-------
                        * * METRIC UNITS  *  *
FILE NAME - 42B
RUN # - 42 - Method 17 Train B for PM
LOCATION - Unit 2A Baghouse Outlet Duct
DATE - 11/20/99 Time: 1350-1512
PROJECT # - 104703.1.002.05.02

Initial Meter Volume  (Cubic Meters)=
Final Meter Volume  (Cubic Meters)=
Meter Factor=
Final Leak Rate  (cu m/min)=
Net Meter Volume  (Cubic Meters)=
Gas Volume (Dry Standard Cubic Meters)=

Barometric Pressure  (mm Hg)=
Static Pressure  (mm H20) =

Percent Oxygen=
Percent Carbon Dioxide=
Moisture Collected  (ml)=
Percent Water=
          PROG.=VER 06/27/89
          11-23-1999  09:17:04
Average Meter Temperature  (C)=
Average Delta H  (mm H20)=
Average Delta P  (mm H20)=
Average Stack Temperature  (C)=

Dry Molecular Weight=
Wet Molecular Weight=

Average Square Root of Delta P  (mm H20)
% Isokinetic=
 5.909
 6.562
 1.010
0.0000
 0.660
 0.641

   761
  -459

   5.1
  14 .1
  60.9
  11.2

    29
   7.4
  22.2
    84

 30.46
 29.06

4.6986
  98.9
Pitot Coefficient=                             0.84
Sampling Time  (Minutes)=                       80.0
Nozzle Diameter  (mm)=                          3.71
Stack Axis #1  (Meters)=                       1.448
Stack Axis #2  (Meters)=                       1.676
Rectangular Stack
Stack Area (Square Meters)=                   2.427

Stack Velocity   (Actual, m/min)=              1,076
Flow rate  (Actual, Cubic m/min)=              2,613
Flow rate  (Standard, Wet, Cubic m/min)=       2,052
Flow rate  (Standard, Dry, Cubic m/min)=       1,821

Particulate Loading - Front Half

Particulate Weight  (g)=                      0.0210
Particulate Loading, Dry Std.  (mg/cu m)=       32.8
Particulate Loading, Actual  (mg/cu m)=         22.8
Emission Rate  (kg/hr)=                         3.57

No Back Half Analysis
          Corr. to 7% 02 & 12% C02
                 28 .8      27.9
                            RCA#2 APPENDIX B
                                                                            77

-------
FILE NAME - 42B
RUN # - 42 - Method  17 Train B  for  PM
LOCATION - Unit 2A Baghouse Outlet  Duct
DATE - 11/20/99 Time: 1350-1512
PROJECT # - 104703.1.002.05.02
Point #

 1
 2
 3
 4
 5
 6
 7
 8
 9
 10
 11
 12
 13
 14
 15
 16
                                  PROG.=VER 06/27/89
                                  11-23-1999  09:17:04
Delta P
(in
0.
0.
0.
0.
1.
0.
0.
0.
0.
0.
0.
0.
1.
0.
0.
0.
. H20)
840
820
850
840
300
780
870
950
950
760
830
670
000
930
970
640
Delta H
(in.
0.
0.
0.
0.
0.
0.
0.
0.
0.
0.
0.
0.
0.
0.
0.
0.
H20)
28
27
28
28
43
26
29
31
32
25
28
22
33
31
32
21
Stack
(F)
184
184
185
185
184
184
183
184
184
183
183
183
185
182
183
183
T Meter T
In(F)
82
82
82
82
83
84
85
85
86
86
87
87
87
88
88
88
Out (F)
81
82
82
82
82
83
83
83
84
84
85
85
86
86
86
87
Fraction

DRY CATCH
FILTER

Fraction

PROBE RINSE
IMPINGERS
Probe Rinse Blank
Impinger Blank  (mg/ml)=  0.0000
 Final Wt.  Tare Wt.  Blank Wt.  Net Wt
  (g)        (g)        (g)       (g)
0.0000    0.0000    0.0000    0.0000
3.3340    3.3140    0.0000    0.0200

 Final Wt.  Tare Wt.    Vol.    Net Wt
  (g)        (g)       (ml)       (g)
3.6897    3.6887    25.4    0.0010
0.0000    0.0000     0.0    0.0000
     =  0.0000
 78
                                RCA#2 APPENDK B

-------
                                            Particulate Matter Concentration Results Converted To Other Units
                       Standard Temperature = 68 °F
Standard Pressure = 29.92 in. Hg
RCA#2
Run Number-
Train Number
30-A
30-B
31-A
31-B
32-A
32-B
33-A
33-B
34-A
34-B
35-A
35-B
36-A
36-B
37-A
37-B
38-A
38-B
39-A
39-B
40-A
40-B
41-A
41-B
42-A
42-B
* 1 l_ :i 	 _i;t; _
PM
collected,
grams
0.0409
0.0335
0.0293
00188
0.0208
0.0142
0.0279
00260
00116
0.0137
0.0144
0.0088
00271
0.0171
0.0512
0.0333
0.0331
0.0222
0.0311
0.0228
0.0107
0.0089
00223
0.0136
0.0346
00210
PM
collected,
mg
409
33.5
29.3
188
20.8
14.2
279
260
11.6
13.7
144
88
27.1
17.1
51.2
33.3
33.1
22.2
31.1
22.8
10.7
8.9
22.3
13.6
346
21.0
Sample
Volume,
dscf
35365
35886
27.394
28.037
26412
28660
34.856
35.334
26.738
28895
25.758
27.751
24.832
26.769
22.534
23.021
22.620
23.379
22.196
23.595
21.591
21.430
22.684
24.054
22.059
22.643
Sample
Volume,
dscm
1.001
1.016
0.776
0794
0.748
0.812
0987
1.001
0757
0.818
0.729
0.786
0.703
0.758
0.638
0.652
0641
0.662
0629
0.668
0.611
0607
0.642
0.681
0.625
0.641
Average
Gas Temp.,
°F
178
180
177
180
177
180
178
180
179
182
179
181
179
182
177
179
177
180
177
179
179
181
180
182
181
184
Barometric
Pressure,
in. Hg
2965
29.65
2960
29.60
29.97
29.97
30.00
30.00
29.96
29.96
30.18
30.18
30.19
30.19
30.20
3020
30.20
30.20
30.20
30.20
30.08
30.08
30.07
30.07
29.98
29.98
Static
Pressure,
in. w.c.
-25.90
-25.90
-26.00
-26.00
-27.12
-27.12
-2685
-26.85
-27.39
-27.39
-25.00
-25.00
-25.91
-25.91
-1709
-17.09
-17.08
-17.08
-16.15
-16.15
-17.10
-17.10
-18.10
-18.10
-18.07
-18.07
Gas
Pressure,
in. Hg
27.75
27.75
27.69
27.69
27.98
27.98
28.03
28.03
27.95
27.95
28.34
28.34
2828
28.28
28.94
28.94
28.94
2894
29.01
29.01
28.82
2882
28.74
28.74
28.65
28.65
Gas
Moisture,
percent
11 1%
1 1 0%
12.2%
1 1 0%
11.3%
11.9%
12.3%
11.6%
13.0%
12.5%
12.0%
11.4%
11.6%
12.5%
10.5%
9.8%
11.4%
10.1%
10.4%
10.3%
12.4%
12.4%
12.4%
12.4%
12.4%
11.2%
PM Loading,
27.85
22.44
25.43
16.08
19.11
11.89
19.21
17.74
10.28
11.25
13.59
7.74
26.60
15.34
57.56
36.82
36.70
24.05
3562
24.52
12.20
10.19
24.09
13.81
38.26
22.83
PM Loading,
mg/dry m3
@ std. temp.*
4046
32.66
37.35
23.42
27.85
17.52
28.33
26.04
15.34
16.76
19.91
11.29
38.87
22.75
80.96
51 54
52.14
33.83
49.92
34.43
17.59
14.74
34.88
2006
5548
32.80
PM Loading,
mg/dscm
40.84
32.97
37.77
2368
27.81
1750
28.27
25.99
15.32
16.74
19.74
11.20
38.54
22.56
8024
51.08
51.68
33.53
49.48
34.12
17.50
14.67
34.72
19.97
5539
32.75
RSD,
10.7%

22.9%

22.8%

4.2%

4.4%

27.6%

26.2%

22.2%

21.3%

18.4%

8.8%

27.0%

25.7%

co
          PMCONV6X.WK4 11/23/99 0850AM

-------
                                    40 CFR 60, APPENDIX A, METHOD 1 -
                        LOCATION OF TRAVERSE POINTS IN A RECTANGULAR DUCT

                MRI Project No.   104703.1.002.05.01
                 Client/Source:   U.S. EPA OAQPS EMAD EMC / Cogentrix Unit 2A
               Source Location:   Rocky Mount, North Carolina
             Sampling Location:   Baghouse (Fabric Filter) Outlet Duct
                         Date:   11/15/99
              For Run Numbers:   All
                       75.4"
                       62.2"
                       49.0"
                       35.8"
                       22.6"
                                     A-5     •
                                   • A-4
                                      A-3
•  A-2
• A-1
                                                                                              as
                                                                                              93
                                                           o
                                                           c
                                                                                              CO
                                                                                              (O
                                             B
                               D
                                                     57 inches

                                          Compass Direction  ^"  North

                                   Flow is away from observer and is downward
                     Inside of far wall to outside of port (Distance A):
                    Inside of near wall to outside of port (Distance B):
                                          Traverse distance (A - B):
                         Internal duct dimension normal to traverses:
                                              Equivalent diameter:
                                       Cross-sectional area of duct:
                                             Number of test ports:
                                     Distance between port centers:
            Distance of nearest flow disturbance upstream from ports:
         Distance of nearest flow disturbance downstream from ports:
                    Number of test points per traverse (i.e., per port):
                         Distance between test points on a traverse:
         Dimensions obtained by/from: direct measurements and  blueprints

                    Data recorded by:  D. Griffin
         COMMENTS:
82.0
16.0
66.0
57.0
61.17
26.125
5
11.4
82
128
5
13.2
inches
inches
inches
inches
inches
square feet

inches
inches
inches

inches
         DUCTR6CT.WPD October 14, 1998 (rev. DUCTREC3.WPD November 10, 19991
80
                                            RCA#2 APPENDIX B

-------
                                             METHOD 5 METERING CONSOLE QUALITY CONTROL CHECK
                                              MRI Project No.
                                         Metering Console No.
                                      Dry Gas Meter Factor (Y):
                                 Orifice Meter Delta-H @, in. w.c.
                                     Barometric Pressure, in. Hg
104703.1.002.05.
     N-12
     0.996
     1.810
     30.00
   Date:
Operator:
11/16/99
C. Clapsaddle
n
£
KJ

Run 1
Final
Initial
Run 2
Final
Initial
Run 3
Final
Initial
Time, i!
seconds
Dry Gas
.Meter , ,
Volume, ,
ft.s
, ; Orifice
- , Meter
	 ' f-\_ li*» • 1 f •.•' 	 !. ,1
, Delta-H, ,
' in, w.c,
'; Dry Gas
Meter Jnlet
Temperature,
°F
Dry Gas
Meter Outlet
Temperature,
. ,"°F'
Dry Gas
, Meter
Factor •
(Yc)


600
0
600
299.606
292.193
7.413
1.81
~ 1.81
1.81
59
54
52
52
514 °R

600
b
600
307.064
299.606
7.458
1.81
1.81
1.81
62
58
53
53
516 °R





- -

	 --
- - 	 	
°R
0.997
0.993

Average Yc: 0.995
Acceptability Criterion: 0.97Y < Yc < 1.03Y
QC Check Result. Metering Console Is Acceptable
  00
                                 M5QCHECK.WK4 11/01/99  (rev. N12QCHK.WK4 11/23/99 08:49 AM)

-------
                                        Alternative Method 5 Post-Test Calibration
                        MRI Project No.  104703.1.002.05.01
                     Sampling Location:  Unit 2A Baghouse Outlet	
                               Run No.   30-TrnA   Run Date:   11/16/99
Console No.     N-12
data
line
1
2
3
4
5
6
7
8
9
10
11
12
13
14
15
16
17
18
19
20
21
22
23
24
25
26
27
28
29
30
31
32
33
34
35
36
37
38
39
40
41
42
43
44
45
46
47
48
Orifice
delta H
0.72
0.69
0.53
0.20
0.01
0.78
0.75
0.66
0.24
0.03
0.79
0.79
0.76
0.47
0.07
0.76
0.72
0.69
0.38
005
0.73
0.67
0.57
0.21
0.03























sqrt
delta H
0.84853
0.83066
0.72801
0.44721
0.10000
0.88318
0.86603
0.81240
0.48990
0.17321
0.88882
0.88882
0.87178
0.68557
0.26458
0.87178
0.84853
0.83066
0.61644
0.22361
0.85440
0.81854
0.75498
0.45826
0.17321
DGM temperature (tm)
inlet, "F
51
52
53
53
54
53
54
55
57
57
55
57
58
59
59
58
58
60
60
60
59
61
61
62
61























outlet, "F
51
52
53
52
53
53
53
54
54
54
54
55
55
55
56
56
56
57
57
57
58
58
58
58
58























                                                                       DGM delta H@:
                                                                                         1.81  in. w.c.
                                                                       Orifice delta H (average):
                                                                                      0.49200  in. w.c.

                                                                       sqrt delta H (average):
                                                                                      0.64916

                                                                       DGM temperature (average):
                                                                                       515.75  °R

                                                                       Barometric pressure:
                                                                                        29.65  in. Hg

                                                                       Dry gas molecular weight (Md):
                                                                                        30.58  Ib/lb-mole
                                                                       Total sampling time'
                                                                                          100  minutes
                                                                       Sample volume (unconnected)
                                                                       as read on DGM:
                                                                                       34.993 dcf

                                                                       DGM correction factor (Y):
                                                                                        0.996

                                                                               Yqa     0.9990

                                                                         Difference      0.30%

                                                                            Result:    PASS
                    YQA48PT.WK4 10/19/99 (rev. YQAN12.WK4  11/23/99 08:52 AM)
                            Page 1
82
                                              RCA#2 APPENDIX B

-------
                                             METHOD 5 METERING CONSOLE QUALITY CONTROL CHECK
                                             MRI Project No.
                                         Metering Console No.
                                      Dry Gas Meter Factor (Y):
                                Orifice Meter Delta-H @, in. w.c.
                                    Barometric Pressure, in. Hg
                           104703.1.002.05.
                                 N-11
                                1.010
                                1.898
                                30.00
   Date:
Operator:
11/16/99
C. Clapsaddle
n
S
m
w




,
, ,
Time, '
seconds
Dry Gas '
Meter , ,:;
Volume; :
ft,s
, ..Orifice, , , „
, Meter
, Delta-H, '
in, w.c.
•, Dry Gas,
, Meter Inlet
Temperature,
,. ', "F -.
, Dry Gas ,;
Meter Outlet
Temperature;
-•• °F'.' '•
,- Dry Gas
, Meter,
Factor
(Vc)

Run 1
Final
Initial

600
0
600
932.994
925.421
7.573
1.90
1.90
1.90
64
60
60
58
520 °R


0.982
Run 2
Final
Initial

600
0
600
940.462
932.994
7.468
1.90
1.90
1.90
65
63
60
60
522 °R


0.997
Run 3
Final
Initial














°R



Average Yc: 0.990
Acceptability Criterion: 0.97Y < Yc < 1.03Y
QC Check Result: Metering Console Is Acceptable
  CO
  CO
M5QCHECK.WK4  11/01/99 (rev. N11QCHK.WK4 11/23/99 08:46 AM)

-------
                                       Alternative Method 5 Post-Test Calibration
                        MRI Project No.
                     Sampling Location:
                              Run No.
1047031.002.05.01
Unit 2A Baghouse Outlet	
 30-TrnB   Run Date:   11/16/99
Console No.     N-11
data
line
1
2
3
4
5
6
7
8
9
10
11
12
13
14
15
16
17
18
19
20
21
22
23
24
25
26
27
28
29
30
31
32
33
34
35
36
37
38
39
40
41
42
43
44
45
46
47
48
Orifice
delta H
0.85
0.81
0.68
0.35
0.05
0.78
0.65
0.58
0.23
0.03
0.75
0.68
0.58
0.22
0.03
0.75
0.71
0.68
0.30
0.04
0.88
0.85
0.75
0.55
0.04 	 ,























sqrt
delta H
0.92195
0.90000
0.82462
0.59161
0.22361
0.88318
0.80623
0.76158
0.47958
0.17321
0.86603
0.82462
0.76158
0.46904
0.17321
0.86603
0.84261
0.82462
0.54772
0.20000
0.93808
0.92195
0.86603
0.74162
0.20000




DGM temperature (tm)
inlet, °F outlet, °F
54
54
55
55
55
55
55
56
57
57
57
58
57
58
58
58
58
59
59
60
59
59
61
62
62























53
54
54
55
55
55
55
55
56
56
56
57
56
57
57
57
57
58
58
58
59
59
60
60
60























                                                                       DGM delta H@:
                                                                                        1.898 in. w.c.
                                                                       Orifice delta H (average):
                                                                                      0.51280 in. w.c.

                                                                       sqrt delta H (average):
                                                                                      0.66435

                                                                       DGM temperature (average):
                                                                                       516.77 °R

                                                                       Barometric pressure:
                                                                                        29.65 in. Hg

                                                                       Dry gas molecular weight (Md):
                                                                                        30.58 !b/lb-mole
                                                                       Total sampling time:
                                                                                          100 minutes
                                                                       Sample volume (uncorrected)
                                                                       as read on DGM:
                                                                                       35.084 dcf

                                                                       DGM correction factor (Y):
                                                                                        1.010

                                                                               Yqa     0.9967

                                                                         Difference     -1.31%

                                                                            Result:    PASS
                    YQA48PT.WK4  10/19/99 (rev. YQAN11.WK4  11/23/99 08:51 AM)
                                                             Page 1
84
                                              RCA#2 APPENDIX B

-------
               ON SITE MERCURY BAROMETER READING CORRECTION
         AND ANEROID BAROMETER CALIBRATION CHECK AT TEST LOCATION

   Mercury Barometer Description:  Princo Model 453, S/N W13559
     Mercury Barometer Location:  Plant Control Room

       Distance Of Barometer From Test Site:        0.00 miles
      Altitude Of Barometer Above Sea Level:       124.0 feet
                           Latitude (north):          36 degrees,         0.00 minutes

                       Facility:  Cogentrix of Rocky Mount, North Carolina

  Test Site And Sampling Location:  Unit 2A Baghouse Outlet Duct

                          MRI Project No.   104703.1.002.05.01
                                   Date:   11/21/99
                                   Time:   0958

                     Readings Obtained By:   J. Surman              y^'

              Observed Barometer Reading:       30.20 in. Hg

              Mercury Column Temperature:          74 °F

                Correction For Temperature:        -0.12 in. Hg

         Reading Corrected For Temperature:       30.08 in. Hg

                     Correction For Gravity:        -0.03 in. Hg

    Temperature Corrected Reading Corrected For Gravity:       30.05  in. Hg


                Aneroid Barometer I.D. No.:     Y-2101

                Reading Before Adjustment:       30.03 in. Hg

                   Calibration Check Result:   within 0.1 in. Hg

                  Reading After Adjustment:   	 in. Hg
Remarks:
BAROMETR.WK4  10/19/98 (rev. BAR04703.WK4  11/23/99 08:37 AM)
                                                                                         85
                     RCA#2 APPENDIX B

-------
                                 RCA #2 Appendix C
                    M17 Field Sampling Data Sheets
MRJ-OPPT\R4703-02-07 Appendices Covers WPD

-------
                                                                FIELD SAMPLING DATA FOR METHOD 17 TRAINS
I
KJ
H
o
Run No.
                                 Dale
                Projecl No.   104703.1.002.05.01
                Clienl U.S. EPA OAQPS EMAD EMC
                Source  Cogenlrix Unil 2A _
                Sampling Localion Baghouse Outlet
                Operator
                Record dala every
                Baromeler No.  Y-2021
                    t
 minules
                Baromelric Pressure
                Elevation lo Meier Boxes
                Meier Box  P,
	in Hg
 34    fl
                          bar
Elevalion lo Sampling Loc.
Sampling Localion Pbar
Static Pressure —*1*\* •
                           	in Hg
                            34    fl
                             . in Hg
Train A No. M17-A
Probe No. A Lenalh: 1 0 fl
Nozzle No. M17-^ Tip Dia. d.H^ in
Pilol Tube No. A CD 0.84
Slack Thermocouple No. 31 58 A
Filler Holder No. /
Filler Assembly No. r •""/
Impinqer Box No. A- /
Umbilical/lmpinger Hookup UH- 30
Umbilical No. ^f^"\_i <\-*b
Meier Box No. ^Jfij? ^'\L>
DGM Correclion (Y) +#tf\- ^'^^
Orifice Meier AH@ "^ I -ol% * ^

Final
w
ftoM
1
Inilial
(oi^
If
.00 (,
Final Meier Volume
Inilial Meier Volume
Leak Check Volume

Initial


Final


Initial


Final



Final
/m 9
^
, 00^1



Initial






Initial

Trait
Final


Initial


Final


Train B Pilot Tube
Initial
{0^1^

i A Sampling System Leak C
Final






Initial







Final
\^\^>
^h^>
rfecks
Final




Initial


Pressure Measurement System Leak Checks
Final




Initial







Initial


Final


Initial


Final


Inilial Final



Final



•*

Inilial







Final





Time (24 Hr)
Vacuum, in Hg
Leak Rate, cfm
Inilial
(0^
ff1
too\
Final Meter Volume
Inilial Meier Volume
Leak Check Volume
Final
IHil
to
.oof

Initial






Final




Inilial




vt'fn
Mrf
Final




Inilial



tt,0
-------
Run No.
Date
                     Sampling Location  Unit 2A Baahouse Outlet Duct
                     Project No.  104703.1.002.05.01	
                                                                   Operator.
                                                                                   page.
                                                                                              of
                                              Sampling Data for Method 1 7 Train A No.   M1 7-A
 Traverse
  Point
        Sampling
          Time,
          min.
          0
                 Clock
                 Time
                (24-Hr)
                     Dry Gas Meter Reading
                           (VJ, ft3
                     Initial
                         Desired     Actual
     Velocity
       Head
       (Ap),
      in. H20
               Orifice Pressure
                 Differential
                   (AH),
                  in. H20
                                                  Desired   Actual
Stack
Temp.
 (ts),
  °F
Dry Gas Meter
 Temperature
                                                                             Inlet
                                                                                Outlet
               Pump
             Vacuum,
               in. Hg
                                                                     /7V
                                                                            J_L
                                                                                           ef-
                                             Z-Z.
                                                                     /71
         /*-
                                                                    /77
                                  2*9.
                                                      .0 1
                                                                            /v
  D-r
         n
                                                    0.7')
                                             I.)
                                                        •/
        ~tfr
                        •7/
^Z3-
                                                    J&+
                                                                     S7S
                                                                         5*7
                                                    5"
 sr-1
                                                            0,7?
                                                                                           9-
         ft,
                                            z.y
             0.76
                                                                 S77
 ft,
                nrf
 £ f
         tt?
                         t,-?
 A"/
l^t
         It
1^7
                                                    0-18-
                                      
                                                                                   5*7
 fl-X
                                             •2.1
                                                            0.6,7
                                                                         &-
                for
                                                     &2-1
                                                                 S7?
                                                                                           •7
         loo
                                                                    /?#•
           r)
                 li/7
                                           Samplinq Data for Method 17 Train B No.   M17-B
                /3J.I
                                                     AM
    V
          f
         JZ-
                                             •7-t
         j£-
                                  #30,
                                                  a.'tf
                                             /.*
                                                                    /71
                                                                    nr
                                                                                   r*
         ~W
                                             &./Z.
                                                                                    •fZ-
                        "Sfoirfr
   V
<2£_
                                                                            5?
                                                                                3*?
                                                                     /av~
                                                                                   &-
 t-
~r
          tt
                                                                                           -7
                                                                    /*2-
                                                     0-75
                                                          L5L£_
                                                                            sv-
         {,$
                fYfr
     ^_
                                              -2..;
                                                                            Ft
                Ml
                                             0,93
                                             -L-7
                                                                                          JO
                                                    0,*S
                                                                                           /O
                <%O-
     i
                                                                                Cff_
Remarks and Notes:
M17DPG2.WPD September 3, 1999
                      Tot:
                      W5I
                                          RCA#2  APPENDIX  C

-------
                      40 CFR 60, APPENDIX A, METHOD 3B
                       INTEGRATED GAS SAMPLING DATA
Run No.
                  Date
Project No.  104703.1.002.05.01	
Sample Type (Multi-Point, Single-Point)
Flow Control Device (Valve, Critical Orifice)
Method 5 Meter Box No.  /
MSB Pump Type  diaphram
MSB Pump No.     /
                       Client/Source U.S. EPA / Coaentrix Unit 2A
                       Sampling Location Unit 2A Baghouse Outlet
                       Operator  <
                                        Bag Type   Tedlar
                                        Method SB Train No._
                                        MSB Flow Meter Type.
                                        MSB Flow Meter No.
                                             Sample No.
                                            NA	
                                                  NA
                                            rotameter
Desired Sampling Rate .
Leak Check Before Sampling.
Total Sampling Time    77
                                  cc/min
Flow Rate, cc/min: Average	
Estimated Total Sample Volume
          O	 After Sampling
         	min  Average Flow Meter Reading
                 	 Highest	
                                                             Lowest
                                          liters
  Time
 (24-Hr)
         Flow
         Meter
        Reading
Start
Purge
  Start
Sampling
  Stop
Sampling
Sampling
Remarks and Notes
          2-0
 tiri
M3BSAMP.WPD June 18. 1998
                            RCA#2 APPENDIX C

-------
I
*
n
                                          40 CFR 60. APPENDIX A, METHOD 3B. GAS ANALYSIS BY ORSAT
                      Run No.
                                  Date
Project No.   104703.1.002.05.01     Sample No. .
Sampling Location  Unit 2A Baghouse Outlet Duct
Analysis Start Time _
                                                                     NA
                      Sample Type (Bag, Grab)
                      Analyst     
3
1 ;93
2 ;9,3
3
Net
Value

X£>-


y.x

2

Actual
Reading
1 s&s
2 /yr'
3
1 J<)3
2 ;9^3
3
Net
Value

S&-


^"•^

3

Actual
Reading
i ;&o
2 ;£".&
3
1 /9&
2 ;9,z
3
Net
Value

/•£>'&


4>Z

Average
Net
Value
(% v/v)

S&".J


y.^.

                                              Acceptance Criteria per Method 3B
                                       C02 >4%  0.3% v/v    O2   >.15%   0.2% v/v
                                            <4%  0.2% v/v          <15%   0.3% v/v
               Remarks and Notes:
               M3BANAL WPD September 3. 1999

-------
               40 CFR 60, APPENDIX A, METHOD 17 - PARTICULATE MATTER TRAIN (M17)
                       FIELD LABORATORY TRAIN SET-UP DATA FOR TWO TRAINS

   MRI Project No. 104703.1.002.05.01
     Client/Source: U.S. EPA OAQPS EMAD EMC / Cogentrix Unit 2A
   Source Location: Rocky Mount, North Carolina
 Sampling Location: Baghouse (Fabric Filter) Outlet Duct
  Run No.   30     Sampling Train A No.
                   Sampling Train B No.
  Set-up person(s): 	
Transfer to Sampler:
Relinquished By     
                  Date/Time
                                     REAGENT
                  LOADING DATA
                                         0$ JO
                                                                           TRAIN A
                                        TRAIN B
       Sampling Nozzle (Quartz)*

     Filter Assembly and Holder*             .
                    Filter Type: Whatman QM-A
                Probe (316 SS)
    Sample Transfer/Vacuum Line
 Male 1st Impinger Inlet Blank-Off
    Nozzle I.D. No.

Fitter Assembly No.

  Fflter Holder No.
         1st Impinger (Mod-GBS) 100-200 mLs ASTM Type I Water
               U-Connector (A)                            .:  .
             2nd  Impinger (GBS) 100-200 mLs ASTM Type I Water
               U-Connector (B)
         3rd Impinger (Mod-GBS) Empty
               U-Connector (C)
         4th Impinger (Mod-GBS) "200 g indicating silica gel
               U-Connector (D)
         5th Impinger (Mod-GBS) "200 g indicating silica gel
       Impinger Outlet Connector
Connector I.D. No.
                        /
                                                                             Initial Weights (grams)
        Before and after sampling: Nozzle inlet opening and filter assembly holder outlet opening covered with Teflon® tape, and
        entire filter assembly holder with filter assembly and nozzle wrapped in aluminum foil and placed in Ziploc® bag. 1 st impinger
        inlet sealed with glass blank-off.
Comments:
M17DSUP.WPD May 13, 1999 (rev. M17DSUP3.WPD November 10, 1999I
                                     RCA#2 APPENDIX  C

-------
              40 CFP 60, APPENDIX A, METHOD 17 - PARTICULATE MATTER TRAIN (M17)
                   FIELD LABORATORY SAMPLE RECOVERY DATA FOR TWO TRAINS
   MRI Project No.  104703.1.002.05.01
     Client/Source:  U.S. EPA OAQPS EMAD EMC / Cogentrix Unit 2A
  Source Location:  Rocky Mount, North Carolina
 Sampling Location:  Baghouse (Fabric Filter) Outlet Duct
Run No.
                  Sampling Train A No.
                  Sampling Train B No.
7-fi
                       Impinger Box A No.
                       Impinger Box B No.
                                                                            ~ J
Transfer for Recovery:
Relinquished By   & &SJTTJSI _  Received By
    Sample recovery person(s):     t/
Weights below are in grams.
                                                                   Date/Time
                                                                                    Date:
                                          BACK HALF RECOVERIES
                            TRAIN A
              1st
 Impinger:
  Final Wt.
 Initial V
   Net Wt.            	
Total Condensate Collected:
Description and/or color:
                      2nd
3rd
 4th & 5th
1st
                                              % Blue
                                                                             TRAIN B
2nd
                                                                                   3rd
                                                                                           4th & 5th
                                                                                        •7/23
                                                                                   A*
                                                                                             % Blue
                                       ..; FRONT HALF RECOVERIES
                            TRAIN A
FILTER ASSEMBLY:
        Sample Number:  3$ 102
    PM Description/color:
TRAIN RINSES:
        Sample Number:
   Components Rinsed*: nozzle, filter holder front
                                                                           TRAIN B
                                                                     104
     * Acetone rinses with brushing 3 times or more until perceivably clean.

COMMENTS: Acetone rinses are transferred directly to tared Teflon® beaker liners for analysis.
M17DRCV.WPD May 13, 1999 (rev. M17DRCV3.WPD November 10. 19991
                                          RCA#2 APPENDIX C

-------
                                                                 FIELD SAMPLING DATA FOR METHOD 17 TRAINS
O
                Run No.
                  Date
Project No.   1 04703.1 .002.05.01
Client  U.S. EPA OAQPS EMAD EMC
Source  Coqentrix Unit 2A _
Sampling Location Baghouse Outlet
Operator   <£r>Tt*'~~ _
Record data every A-3   g-5  minutes
Barometer No.  Y-2021 _
                               in Hg
                            34    ft
                               m Hg
                                  ft
Barometric Pressure   ,2-7-y 3
Elevation to Meter Boxes 	
Meter Box Pbat      '2-%it0
Elevation to Sampling Loc. 	
Sampling Location p.   2-/'<
            .M
                                            34
                               ,
                Static Pressure/
                                              .in Hg
Train A No. M17-A
Probe No. A Lenath: 1 0 ft
Nozzle No. M17-/V Tip Dia. O. /^lf in
Pitot Tube No. A CD 0.84
Stack Thermocouple No. 31 58A
Filter Holder No. ?
Filter Assemblv No. ?''*)
Impinqer Box No. A- 1-
Umbilical/lmoinaer Hookup UH-V /
Umbilical No. A/**?"^
Meter Box No. /uVz_-
DGM Correction (Y) O, 91?//
Orifice Meter AH@ /,$/ '
DGM Correction (Y) /,<5/O
Orifice Meter AH@ /,#?$'
                                                                                                                                                page 1 of,
                                                                                                                                           Y
                                                                                                                                            1  •
                                     Assumed Moisture
                                                                        % Assumed %CO,
       lAJ  LfiJ  LcJ  LoJ  l£j
        Traverse Point Layout
   Compass Direction > North
Nozzles are quartz-glass.

Time (24 Hr)
Pass or Fail
Train A Pitot Tube Pressure Measurement System Leak Checks
Initial
w

Final
ll/W
0°°
Initial


Final


Initial


Final


Initial


Final


Initial


Final


Train B Pitot Tube Pressure Measurement System Leak Checks
Initial
'^

Final
ll
Final Meter Volume
Initial Meter Volume
Leak Check Volume
Final
l^o
?
,oO^

Initial






Final




Initial






Final




Initial






Final




Initial






Final





Time (24 Hr)
Vacuum, in Hg
Leak Rate, cfm
Initial
IW}^
^i
,ooM
Final Meter Volume
Initial Meter Volume
Leak Check Volume
Final
lu«H
-7
,m

Initial






Final




Initial






Final




Initial



IMLrt0!
TJ&Xtf
T--1.1J.O
Final




Initial



^F^.^/2-
VWl'}
2-T.f-r-i
Final




               Remarks and Notes:  List any other equipment requiring calibration below.
                                                                                                              TRAIN A
              M17DPQ1 WPD Seplembei 3, 1999
                                                                               Meter Volume at Start of Run
                                                                                Meter Volume at End of Run
                                                                     Total Leak Check or Non-Sample Volume
                                                                                     Adjusted Final Volume

-------
    No.
Date
             Sampling Location  Unit 2A Baahouse Outlet Duct
             Project No.   104703.1.002.05.01	
                                                                                       page.
                                                                                 of  2—
                                                                    Operator.
                                               Sampling Data for Method 17 Train A No.   M17-A
 Traverse
  Point
        Sampling
          Time,
          min.
        Clock
        Time
        (24-Hr)
        Dry Gas Meter Reading
              (VJ, ft3
        Initial
                         Desired     Actual
Velocity
 Head
 
-------
                      40 CFR 60, APPENDIX A, METHOD 3B
                       INTEGRATED GAS SAMPLING DATA
Run No..
                  Date
Project No.  104703.1.002.05.01	
Sample Type (Multi-Point, Single-Point)
Flow Control Device (Valve, Critical Orifice)
Method 5 Meter Box No._
MSB Pump Type  diaphram
MSB Pump No.	A/2-
                       Client/Source U.S. EPA / Cogentrix Unit 2A
                       Sampling Location Unit 2A Baahouse Outlet
                       Operator
                       Bag Type   Tedlar
                       Method SB Train No._
                       MSB Flow Meter Type.
                       MSB Flow Meter No.
                                                             Sample No.
                                                            NA	
                                                                          NA
                                                             rotameter
Desired Sampling Rate
Leak Check Before Sampling
Total Sampling Time
                                  cc/min
Flow Rate, cc/min: Average	
Estimated Total Sample Volume
            	^_	 After Sampling
            min  Average Flow Meter Reading
            ^- °	 Highest
                                                             3-0
                                                             Lowest
                                          liters
  Time
 (24-Hr)
         Flow
         Meter
        Reading
Start
Purge
                         Start
                        Sampling
  Stop
Sampling
Sampling
Remarks and Notes
 Sfio
         2- ,
        2- -
        1.0-
 tft*
M3BSAMP.WPD June 18. 1998
                            RCA#2 APPENDIX C

-------
s
o
                                           40 CFR 60, APPENDIX A, METHOD 3B, GAS ANALYSIS BY ORSAT
                       Run No.
                                  Date
Project No.  104703.1.002.05.01     Sample No. .
Sampling Location   Unit 2A Baghouse Outlet Duct
Analysis Start Time _
                                                                      NA
                       Sample Type (Bag, Grab)
                       Analyst   c
                         Baa
                             Orsat Leak Check Before Analysis:
                             Burrete    A/v     Change in 4 Minutes
                             Pipettes  tA/e	Change in 4 Minutes
                             Orsat Leak Check After Analysis:
                             Burrete   A/P	Change in 4 Minutes
                             Pipettes  /Y'o     Change in 4 Minutes
Analysis


Gas
C02


O2 (Net is actual reading
minus actual CO2 reading)

1

Actual
Reading
1 W
2 W-b
3
1 /*;
2 /$.<>
3
Net
Value




y,j>

2

Actual
Reading
1 ;*>i
2 /*>,(*
3
1 JJ.&~

3

Actual
Reading
1 /*>£•
2 /V.<£
3
1 ;?.;
2 ;9,J
3
Net
Value

S4/.6'


^^S"

Average
Net
Value
(% v/v)

s&t.


y.i5~

                                               Acceptance Criteria per Method 3B
C02
>4%
<4%
0.3% v/v
0.2% v/v
                                          O2
                                               <15%
                                                                              0.2% v/v
                                                                              0.3% v/v
               Remarks and Notes:
               M3BANAL WPD September 3, 1999

-------
              40 CFR 60, APPENDIX A, METHOD 17 - PARTICULATE MATTER TRAIN (M17)
                       FIELD LABORATORY TRAIN SET-UP DATA FOR TWO TRAINS

   MRI Project No. 104703.1.002.05.01
     Client/Source: U.S. EPA OAQPS EMAD EMC / Cogentrix  Unit 2A
  Source Location: Rocky Mount, North Carolina
Sampling Location: Baghouse (Fabric Filter) Outlet Duct
  Run No.   <3j     Sampling Train A No.  /&J?~S9	  Impinger Box A No..
                   Sampling Train B No.  /^/^-^	  Impinger Box B No..
  Set-up person(s):    'J> St.fr'jrnSr?		   Date:
Transfer to Sampler:
Relinquished By    c/ £us~j7r&t       Received By  £?> 6f' f~T> n	  Date/Time
      TRAIN COMPONENT	REAGENT	LOADING DATA	

                                                                           TRAIN A          TRAIN B

       Sampling Nozzle (Quartz)*                     ;.    Nozzle l.D. No.
                                                                             Initial Weights (grams)
     Filter Assembly and Holder*                     ;  Fitter Assembly No. _
                   Filter Type: Whatman QM»A    . •":
                Probe (316 SS)                     :     Filter Holder No. _
   Sample TransferA/acuum Line            .      • .  ::
 Male 1st Impinger Inlet Blank-Off


         1 st Impinger (Mod-GBS) 100-200 mLs ASTM Type I Water  ..        _
               U-Connector (A)                    .  : ;       .
            2nd Impinger (GBS) 100-200 mLs ASTM Type I Water           _
               U-Connector (B)
         3rd Impinger (Mod-GBS) Empty                                   _
               U-Connector (C)
         4th Impinger (Mod-GBS) "200 g indicating silica gel                 	
               U-Connector (D)
         5th Impinger (Mod-GBS) "200 g indicating silica gel                 	

       Impinger Outlet Connector                        Connector l.D. No. 	

      *  Before and after sampling: Nozzle inlet opening and filter assembly holder outlet opening covered with Teflon® tape, and
        entire filter assembly holder with filter assembly and nozzle wrapped in  aluminum foil and placed in Ziploc® bag.  1 st impinger
        inlet sealed with glass blank-off.


Comments:                                                                 -r? />

                                                                            D////11
M17DSUPWPD May 13, 1999 (rev M17DSUP3.WPD November 10, 1999)
                                                                                                       11
                                     RCA#2 APPENDIX C

-------
                  40 CFR 60, APPENDIX A, METHOD 17 - PARTICULATE MATTER TRAIN (M17)
                       FIELD LABORATORY SAMPLE RECOVERY DATA  FOR TWO TRAINS
       MRI Project No. 104703.1.002.05.01
        Client/Source: U.S. EPA OAQPS EMAD EMC / Cogentrix Unit 2A
      Source Location: Rocky Mount, North Carolina
    Sampling Location: Baghouse (Fabric Filter) Outlet Duct
  Run No.
                      Sampling Train A No.  SW- S9
                      Sampling Train B No.
   Transfer for Recovery:
   Relinquished By   .£?
Received By   t). ~
                                                         Impinger Box A No.
                                                         Impinger Box B No.
                                                                     Date/Time
    Sample recovery person(s):
Weights below are in grams.
                                  t).
                                                                                         Date:
                                             BACK HALF RECOVERIES
                               TRAIN A
                                                                                TRAIN B
Impinger:     1st
Final Wt.
Initial Wt. J
 Net Wt.
                           2nd
                                   3rd
        4th & 5th
                                                                 1st
2nd
                                                                                   3rd
                                                                                                4th & 5th
   Total Condensate Collected:
   Description and/or color:
                                                                                                 "7.2
                                                 % Blue
                                                                                              % Blue
                                             FRONT HALF RECOVERIES
                               TRAIN A
                                                                                TRAIN B
   FILTER ASSEMBLY:                                     :
           Sample Number:  ^^102                                    o?,> 104
       PM Description/color:    fr^^k	               J?)*£j
   TRAIN RINSES:
           Sample Number:  ^]/101                                    &j 103
      Components Rinsed*: nozzle, fitter holder front
        *  Acetone rinses with brushing 3 times or more until perceivably clean.

   COMMENTS: Acetone rinses are transferred directly to tared Teflon® beaker liners for analysis.
   M17DRCV WPD May 13. 1999 (rev. M17DRCV3 WPD November 10, 19991
12
                                             RCA#2 APPENDIX C

-------
I
10
                                                                FIELD SAMPLING DATA FOR METHOD 17 TRAINS
                Run No.
                                  Date
                Project No.   104703.1.002.05.01
                Client  U.S. EPA OAQPS EMAD EMC
                Source  Coaentrix Unit 2A	
                Sampling Location
                Operator   G
                  aahouse Outlet
Record data every A'S
Barometer No.   Y-2021
                                            minutes
                Barometric Pressure 	2L
                Elevation to Meter Boxes
                Meter Box Pha,
                           L__inHg
                            34    ft
Elevation to Sampling Loc.
Sampling Location Pba,   g-
	in Hg
 34    ft
Static Pressure/y ^"^ "•
   . in Hg
Train A No. M17-A
Probe No. A Lenath: 10 ft
Nozzle No. M17- 9 Tip Dia. 0,lW in
Pitot Tube No. A CD 0.84
Stack Thermocouple No. 3158A
Filter Holder No. /"
Filter Assembly No. pf
Impinger Box No. A- /
Umbilical/lmpinaer Hookup UH- Tti
Umbilical No. /V &- V
Meter Box No. /V/2-
DGM Correction IY) £>* ?%
Orifice Meter AH@ /. }?JO
TrainB No. M17-B
Probe No. B Lenath: 10 ft
Nozzle No. M17-/£>Tio Dia. ^-I^Ue in
Pitot Tube No. B C_ 0.84
Stack Thermocouple No. 31 58B
Filter Holder No. £
Filter Assembly No. f (s
Impinqer Box No. B- (
Umbilical/lmpinqer Hookup UH- TZ-
Umbilical No. /^^- 1
Meter Box No. A/ '~ ^
DGM Correction (Y) S^/0
Orifice Meter AH@ /- ??#
Assumed Moisture
                                                             //
                                                                                                                                               page 1 of
                                                                                               1
%  Assumed %CO2
                                                                l">
                                                                                                 %O2
       lAl  LBj  Ld   LfiJ  l£j
        Traverse Point Layout
   Compass Direction s* North
Nozzles are quartz-glass.

Time (24 Hr)
Pass or Fail
Train A Pitot Tube Pressure Measurement System Leak Checks
Initial
ffl\

Final
ion
Sl&QO
1*
Initial


Final


Initial


Final


Initial


Final


Initial


Final


Train B Pitot Tube Pressure Measurement System Leak Checks
Initial
$?3J>

Final
ioM
c&ss>
Initial


Final


Initial


Final


Initial


Final


Initial


Final


O
                                                                      Train A Sampling System Leak Checks

Time (24 Hr)
Vacuum, in Hg
Leak Rate, cfm
Initial
Cflftls
ti
,0o<\
Final Meter Volume
Initial Meter Volume
Leak Check Volume
Final
\Q\°(
7


Initial






Final




Initial






Final




Initial






Final




Initial






Final





Time (24 Hr)
Vacuum, in Hg
Leak Rate, cfm
Initial
08"57
/£
Jo'h
Final Meter Volume
Initial Meter Volume
Leak Check Volume
Final
\Q^>
2
.no^

Initial






Final




Initial






Final




Initial



W'&f
W"fll
1f.1ff
Final




Initial



Itlr t»f
rtlrfll
27.^3^
Final




   CO
               Remarks and Notes:  List any other equipment requiring calibration below.
                                                                                                             TRAIN A
               M17DPQ1 WPD Septembers, 1999
                                                                              Meter Volume at Start of Run
                                                                               Meter Volume at End of Run
                                                                    Total Leak Check or Non-Sample Volume
                                                                                    Adjusted Final Volume

-------
   Run No.
   Date
             Sampling Location  Unit 2A Baohouse Outlet Duct
             Project No.   104703.1.002.05.01	
                                                                       Operator  C^v ft?-—
                                                               page.
                                                                          of
                                                  Sampling Data for Method 17 Train A No.  M17-A
    Traverse
     Point
           Sampling
             Time,
             min.
        Clock
        Time
        (24-Hr)
Dry Gas Meter Reading
      ,
  °F
Dry Gas Meter
 Temperature
                                                                                 Inlet
                                                                            Outlet
               Pump
             Vacuum,
               in. Hg
Silica Gel
Impinger
 Outlet
 Temp.,
   °F
    A-f
        efrft
          2*7 S&
                                                        a
                                            0,6
                                          7(3
             tf
                                                                         //7
                                                                                                       -5.4
                                           2.7
                                     2-0
                            •2.7 ?;
                                                                                                        7V
        2.
 2-7
                                      •2.-7-7-Z/
            -if
                                                             /77_
                                                                                        vs


                                                                        Z2£_
                                                                        /77
             3"'
                                                                        /77
                            rt.70
                                                                                T/
                                                                            y?*
                                                Z-Y
                                              T'S
                                                -2,3
       2-
72-
                   /of*
            75
                                                                    ft
                                                  Sampling Data for Method 17 Train B No.   M17-B
                           twit
                                                             fit?
                                      . VX
                                                                                      52
   Remarks and Notes:
   M17DPG2.WPD September 3. 1999
14
                                             RCA#2  APPENDIX C

-------
                      40 CFR 60, APPENDIX A, METHOD 3B
                       INTEGRATED GAS SAMPLING DATA
                 Date   X/-/7-ff
Run No._
Project No.  104703.1.002.05.01	
Sample Type (Multi-Point, Single-Point)
Flow Control Device (Valve, Critical Orifice)
Method 5 Meter Box No.   /1//2-	
MSB Pump Type  diaphram	
MSB Pump No.
                                        Client/Source U.S. EPA / Coaentrix Unit 2A
                                        Sampling Location Unit 2A Baghouse Outlet
                                        Operator	
                                       Bag Type  Tedlar
                                       Method SB Train No._
                                       MSB Flow Meter Type.
                                       MSB Flow Meter No. _
                                                              Sample No.
                                                            NA	
                                                         NA
                                                             rotameter
Desired Sampling Rate	
Leak Check Before Sampling.
Total Sampling Time	^
                                  cc/min
Flow Rate, cc/min: Average _
Estimated Total Sample Volume
            ^	 After Sampling
            min  Average Flow Meter Reading
                	 Highest	^
                                                             Lowest
                                          liters
 Time
 (24-Hr)
         Flow
         Meter
        Reading
Start
Purge
                          Start
                        Sampling
  Stop
Sampling
Sampling
Remarks and Notes
         "1.
M3BSAMP WPD June 18. 1998

                                                                                    15
                            RCA#2 APPENDIX C

-------
 o>

o
                                           40 CFR 60, APPENDIX A, METHOD 3B, GAS ANALYSIS BY ORSAT
                       Run No.
                                  Date
Project No.  104703.1.002.05.01     Sample No. .
Sampling Location   Unit 2A Baghouse Outlet Duct
Analysis Start Time .
                                                                      NA
                       Sample Type (Bag, Grab)
                       Analyst    c
                         Baa
   Orsat Leak Check Before Analysis:
   Burrete   xVfr	Change in 4 Minutes
   Pipettes  «/K>	Change in 4 Minutes
   Orsat Leak Check After Analysis:
   Burrete   /&	Change in 4 Minutes
   Pipettes  /y&      Change in 4 Minutes
Analysis


Gas
CO2

02 (Net is actual reading
minus actual CO2 reading)

1

Actual
Reading
1 M-7
2 S&7
3
2 /9£'
3
Net
Value
Stf.7

4.$-

2

Actual
Reading
\'%
3
2 ;9sf
3
Net
Value
yy.7

*j

3

Actual
Reading
1 /V.7
3
2 ;$A£~
3
Net
Value
,*•*

**

Average
Net
Value
(% v/v)
;*7

«f

                                               Acceptance Criteria per Method 3B
                                        C0
                             0.3% v/v
                             0.2% v/v
0.2% v/v
0.3% v/v
                Remarks and Notes:
               M3BANAL.WPD Septembers, 1999

-------
               40 CFR 60, APPENDIX A, METHOD 17 - PARTICULATE MATTER TRAIN (M17)
                       FIELD LABORATORY TRAIN SET-UP DATA FOR TWO TRAINS

    MRI Project No. 104703.1.002.05.01
     Client/Source: U.S. EPA OAQPS EMAD EMC / Cogentrix Unit 2A
   Source Location: Rocky Mount, North Carolina
 Sampling Location: Baghouse (Fabric Filter) Outlet Duct
  Run No. <3£Z     Sampling Train A No.  ^yy-^	  Impinger Box A No.
                   Sampling Train B No.  S3?/J7-{3	  Impinger Box B No.
  Set-up person(s):    «-/. £iJ/s&>&s?	   Date:
Transfer to Sampler:
Relinquished  By     **• £*Js'/??l>si       Received By  ^ &sSrr"~>	  Date/Time _,
      TRAIN COMPONENT	REAGENT	LOADING DATA	

                                                                           TRAIN A           TRAIN B

       Sampling Nozzle (Quartz)*                     I     Nozzle I.D. No.   /*}*?->>

     Filter Assembly and Holder*                       Fitter Assembly No. 	
                    Filter Type: Whatman Qft/t-A      \  .                \
                Probe (316 SS)                     :     Filter Holder No. 	  	
    Sample Transfer/Vacuum Line           :          ;                  !
 Male 1st Impinger Inlet Blank-Off                                       ;
                                                                    j         Initial Weights (grams)
         1st Impinger (Mod-GBS) 100-200 mLs ASTM Type I Water  .         _
               U-Connector (A)
            2nd Impinger (GBS) 100-200 mLs ASTM Ty:pe t Water           _
               U-Connector (B)
         3rd Impinger (Mod-GBS) Empty                                  _
               U-Connector (C)
         4th Impinger (Mod-GBS) "200 g indicating silica gel                 	
               U-Connector (D)
         5th Impinger (Mod-GBS) "200 g indicating silica gel                 	

       Impinger Outlet Connector                        Connector I.D. No. 	

     *  Before and after sampling: Nozzle inlet opening and filter assembly holder outlet opening covered with Teflon® tape, and
        entire filter assembly holder with filter assembly and nozzle wrapped in aluminum foil and placed in Ziploc® bag. 1 st impinger
        inlet sealed with alass blank-off.
Comments:
                                                                                    /
                                                                                lirlfi
M17DSUPWPD May 13, 1999 (rev M17DSUP3.WPD November 10. 1999)
                                                                                                       17
                                     RCA#2 APPENDIX C

-------
                 40 CFR 60, APPENDIX A, METHOD 17 - PARTICULATE MATTER TRAIN (M17)
                       FIELD LABORATORY SAMPLE RECOVERY DATA  FOR TWO TRAINS
       MRI Project No. 104703.1.002.05.01
        Client/Source: U.S. EPA OAQPS EMAD EMC / Cogentrix Unit 2A
      Source Location: Rocky Mount, North Carolina
    Sampling Location: Baghouse (Fabric Filter) Outlet Duct
     Run No.
                  Sampling Train A No.
                  Sampling Train B No..
Transfer for Recovery:
Relinquished By   £?• &si ^rjr>
    Sample recovery person(s):
Weights below are in grams.
Received By  cA
                                                             Impinger Box A No..
                                                             Impinger Box B No..
                                                                        Date/Time
          S/0e>
                                                                                         Datp-
                                             BACK HALF RECOVERIES
                               TRAIN A
Impinger:     1st
Final Wt.  7&&?7
Initial Wt.  &'^'S'
 Net Wt.
                           2nd
                                   3rd
        4th & 5th
                                                                 1st
Total Condensate Collected:
Description and/or color:
                                                      frtft'
                                                 % Blue
                                                                                TRAIN B
                                                                         2nd
3rd
                                                                                                4th & 5th
                                                                                                 £3.3
                                                                                                    •?*
                                                                                                      ,%
                                                                                              % Blue
                                             FRONT HALF RECOVERIES
                               TRAIN A
   FILTER ASSEMBLY:
           Sample Number:  ^3^102
       PM Description/color:
   TRAIN RINSES:
           Sample Number:
      Components Rinsed*: nozzle, filter holder front
                                                                                TRAIN B
        * Acetone rinses with brushing 3 times or more until perceivably clean.

   COMMENTS: Acetone rinses are transferred directly to tared Teflon® beaker liners for analysis.
   M17DRCV.WPD May 13, 1999 (rev. M17DRCV3.WPD November 10, 1999)
18
                                             RCA#2 APPENDIX C

-------
                                                                FIELD SAMPLING DATA FOR METHOD 17 TRAINS
g
to
fc
r>
Run No..	
Project No.   104703.1.002.05.01
Client  U.S. EPA OAQPS EMAD EMC
Source  Coaentrix Unit 2A	
Sampling Location-, Baohouse Outlet
Operator.
              •fKl A   1     S - tt,
                              mutes
                                          r" mi
                               Y-2021
                                              in Hg
                                            34    ft
Record data ev
Barometer No..
Barometric Pressure    %
Elevation to Meter Boxes
Meter Box Pba, 	/}p,OO    jn Hg
Elevation to Sampling Loc.     34    ft
Sampling Location^3,,.,,   'jOrOG  jn Hg
Static
Train A No. M17-A
Probe No. A Lenath: 1 0 ft
Nozzle No. M17- f^Tm Dia. O-iHk in
Pitot Tube No. A CD 0.84
Stack Thermocouple No. 31 58A
Filter Holder No. ~1
Filter Assembly No. £*^
Impinger Box No. A- ^
Umbilical/lmpinqer Hookup UH-
Umbilical No. fJ^O -4
Meter Box No. A/ \T-
DGM Correction (Yl 3*fL> in
Pitot Tube No. B C. 0.84
Stack Thermocouple No. 31 58B
Filter Holder No. &
Filter Assembly No. r'-'tf
Impinaer Box No. B- Z~
Umbilical/lmpinqer Hookup UH-'2-
Umbilical No. /l/"?^'/
Meter Box No. /v' / /
DGM Correction (Y) / -* North
Nozzles are quartz-glass.

Time (24 Hr)
Pass or Fail
Train A Pitot Tube Pressure Measurement System Leak Checks
Initial
11 If

Final
I'M
J36^>
Initial


Final


Initial


Final


Initial


Final


Initial


Final


Train B Pitot Tube Pressure Measurement System Leak Checks
Initial
Illtf

Final
fW/

Initial


Final


Initial


Final


Initial


Final


Initial


Final


                                                                      Train A Sampling System Leak Checks

Time (24 Hr)
Vacuum, in Hg
Leak Rate, cfm
Initial
m
.5
.w\
Final Meter Volume
Initial Meter Volume
Leak Check Volume
Final
\VHJ
fl
,00\

Initial






Final




Initial






Final




Initial






Final




Initial






Final





Time (24 Hr)
Vacuum, in Hg
Leak Rate, cfm
Initial
(11-0
.5
•fl(K
Final Meter Volume
Initial Meter Volume
Leak Check Volume
Final
vw
1
.00?)

Initial






Final




Initial






Final




Initial



V/.Ht-
7.'^
W.nt
Final




Initial



Vt.
-------
      Run No.
      Date  /
             Sampling Location  Unit 2A Baahouse Outlet Duct
             Project No.   104703.1.002.05.01	
                                                                           Operator.
                                                                page.
                                                                           of 2-
                                                      Sampling Data for Method 17 Train A No.   M17-A
       Traverse
        Point
              Sampling
                Time,
                min.
         Clock
         Time
        (24-Hr)
Dry Gas Meter Reading
       (VJ, ft3
Initial
                                Desired
                            Actual
Velocity
 Head
 (Ap),
in. H20
Orifice Pressure
  Differential
    (AH),
   in. H20
                                                            Desired   Actual
Stack
Temp.
 (ts),
Dry Gas Meter
 Temperature
    (U,
     °F
                                                                       Inlet   Outlet
 Pump
Vacuum,
 in. Hg

                                                    2,7
                                                                                                    "
          ¥
                                                                            /So
                       It
                                                                      ,o f
                                             &.
                                                                                            5V
                                                            a.%,
                                                                                                    -
                                                                                                    7
                       v-n
               yy
                       I2Z?
                                                    31
                                                                            /7T
                                                                      t-l
               60
      A -
                                             0,72-
                      (Kit
                                                                    
                                                                                                    T
          Z
 52
                                      0, -27
                         /77
                                                                      '*"?
                               :.^
                                                                                                    r
               of
                                             0-72-
                71.
         4.
 -76
                                             OL
pot
                               $61,20
                                                     0,0%
Ft
                                                     IZ£.
          V
                                     2. ,-
                                                               /ft
                                                                      '9
                       CM
                                             a. 75"
                                     0,15
                                 -7$
                                                                             //y
               /oo
                                                                                    S"
      Remarks and Notes:
      M17DPG2WPD September 3. 1999
   20
                                                 RCA#2 APPENDIX C

-------
                       40 CFR 60, APPENDIX A, METHOD 3B
                        INTEGRATED GAS SAMPLING DATA
Run No..
                  Date
Project No.  104703.1.002.05.01	
Sample Type (Multi-Point, Single-Point)
Flow Control Device (Valve, Critical Orifice)
Method 5 Meter Box No.     tf/T,	
MSB Pump Type  diaphram
MSB Pump No.	
                       Client/Source U.S. EPA / Coqentrix Unit 2A
                       Sampling Location Unit 2A Baahouse Outlet
                       Operator	
                                        Bag Type  Tedlar
                                        Method 3B Train No. _
                                        MSB Flow Meter Type.
                                        MSB Flow Meter No.
                                                              Sample No.
                                                             NA	
                                                         NA
                                                             rotameter
Desired Sampling Rate	
Leak Check Before Sampling.
Total Sampling Time     ffi?
                                   cc/min
Flow Rate, cc/min: Average	
Estimated Total Sample Volume
            	 After Sampling
            min  Average Flow Meter Reading
             J**       Highest	
                                                             Lowest
                                           liters
  Time
 (24-Hr)
         Flow
         Meter
        Reading
Start
Purge
                          Start
                        Sampling
  Stop
Sampling
Sampling
Remarks and Notes
 Utf
 tfft
         V
                                                  r efi
M3BSAMP.WPD June 18, 1998
                                                                                    21
                           RCA#2 APPENDIX C

-------
  ro
n
*
to
fc
"a
w
R
o
                                             CFR 60, APPENDIX A, METHOD 3B, GAS ANALYSIS BY ORSAT
                      Run No.
                                  Date
Project No.  104703.1.002.05.01     Sample No. .
Sampling Location   Unit 2A Baghouse Outlet Duct
Analysis Start Time
                                                                      NA
                      Sample Type (Bag, Grab)
                      Analyst   J.
                         Bag
                             Orsat Leak Check Before Analysis:
                             Burrete    tfo	Change in 4 Minutes
                             Pipettes   A£»	Change in 4 Minutes
                             Orsat Leak Check After Analysis:
                             Burrete    Afe      Change in 4 Minutes
                             Pipettes   Svv      Change in 4 Minutes
Analysis


Gas
C02


O2 (Net is actual reading
minus actual CO2 reading)

1

Actual
Reading
1 S*~*
2 /&*/
3
1 Sf.7
2/^.7
3
Net
Value
'



3. '3

2

Actual
Reading
1 A£7y
2 }£~.^
3
1 ;Y


3,3

Average
Net
Value
(% v/v)

'


3.3

                                               Acceptance Criteria per Method 3B
C0
    ,<4%
0.3% v/v
0.2% v/v
                                          02
                                               <15%
                                                                             0.2% v/v
                                                                             0.3% v/v
               Remarks and Notes:
               M3BANALWPD September 3, 1999

-------
              40 CFR 60, APPENDIX A, METHOD 17 - PARTICULATE MATTER TRAIN (M17)
                      FIELD LABORATORY TRAIN SET-UP DATA FOR TWO TRAINS

   MRI Project No. 104703.1.002.05.01
    Client/Source: U.S. EPA OAQPS EMAD EMC / Cogentrix Unit 2A
  Source Location: Rocky Mount, North Carolina
Sampling Location: Baghouse (Fabric Filter) Outlet Duct

                                                 	   Impinger Box A No.    /*"*<	
                                                 	   Impinger Box B No.    &•"&•
  Run No.  33    Sampling Train A No.
                  Sampling Train B No.
  Set-up person(s):  	c/. t$t>^v^rr^^?
Transfer to Sampler:
Relinquished By     
                                                                              Date:
                                                                     Date/Time
      TRAIN COMPONENT
                                    REAGENT
LOADING DATA
                                                                          TRAIN A
                                                                                            TRAIN B
      Sampling Nozzle (Quartz)*

     Filter Assembly and Holder*
                   Filter Type: Whatman QM>A
                Probe  (316 SS)
   Sample Transfer/Vacuum Line           :
 Male 1st Impinger Inlet Blank-Off
                                                       Nozzle I.D. No.

                                                    Fitter Assembly No.

                                                   :   Filter Holder No.
         1st Impinger (Mod-GBS) 100-200 mLs ASTM Type I Water
               U-Connector (A)                 •   =_ .  •
            2nd Impinger (GBS) 100-200 mLs ASTM Type I Water
               U-Connector (B)
         3rd Impinger (Mod-GBS) Empty
               U-Connector (C)
         4th Impinger (Mod-GBS) "200 g indicating silica gel
               U-Connector (D)
         5th Impinger (Mod-GBS) "200 g indicating silica gel
       Impinger Outlet Connector
                                                    Connector I.D. No.
                                                                            Initial Weights (grams)
                                                                                            •73#,
        Before and after sampling: Nozzle inlet opening and filter assembly holder outlet opening covered with Teflon® tape, and
        entire filter assembly holder with filter assembly and nozzle wrapped in aluminum foil and placed in Ziploc® bag.  1 st impinger
        inlet sealed with glass blank-off.
Comments:
                                                                                  ///#•/?*
M17DSUP.WPD May 13, 1999 (rev. M17DSUP3.WPD November 10, 19991
                                                                                                       23
                                     RCA#2  APPENDIX C

-------
                  40 CFR 60, APPENDIX A,  METHOD 17 - PARTICULATE MATTER TRAIN (M17)
                       FIELD LABORATORY SAMPLE RECOVERY DATA FOR TWO TRAINS

       MRI Project No. 104703.1.002.05.01
        Client/Source: U.S. EPA OAQPS EMAD EMC / Cogentrix Unit 2A
      Source Location: Rocky Mount, North Carolina
    Sampling Location: Baghouse (Fabric Filter) Outlet Duct
  Run No.
                      Sampling Train A No.
                      Sampling Train B No.
Transfer for Recovery:
Relinquished By  Z?- £>sjr~T'''S?
    Sample recovery person(s):
Weights below are in grams.
                                        Received By  <)• 
-------
                                                               FIELD SAMPLING DATA FOR METHOD 17 TRAINS
I
a
o
                                                                                                                                            page 1 of.
/rj
Run No. 77
Date /7"/7-?f
Project No. 104703.
1.002.05.01
Client U.S. EPA OAQPS EMAD EMC
Source Coaentrix Unit 2A
Sampling Loce
Operator 6j
Record data e
Barometer No
Barometric Pre
Elevation to IV
Meter Box Pb3I
Elevation to S
Sampling Loce
Static Pressur
Time (24 Hr)
Pass or Fail
tion Baahouse


i/erv 1^1 & ^

Outlet




minutes
Y-20?1
assure
23 o
eter Boxes

ampling
tion Pba,
B.^fe
1f\,%
Loc.

1 in
34
in
34
ifc in
Hg
ft
Hg
ft
Hg
^-#7,3? inH,0
Train A No. M17-A
Probe No.
A
Nozzle No. Ml 7-
Pitot Tube No.
Le
^.Tip
A
Stack Thermocouple No.
Filter Holder No. /
Filter Assembly h
Impinger Box No.
Umbilical/Impinge
Umbilical No.
lo. ?
A-
r Hooki
/(^-
>ngth: _
Dia. 9, /
CP
10 ft
yl/ in
0.84

3158A

-*?
(
JD UH-
y



*)0






Meter Box No. A /2-~
DGM Correction (Y) O.'i'Mt
Orifice Meter AH<3> 1- $!&
Assumed
Moisture
a
Train B No.
Probe No.
Nozzle No._
Pitot Tube h
Stack Them
Filter Holde
Filter Assen
Impinger Bo
Umbilical/In
Umbilical N
Meter Box I
DGM Corre
Orifice Met<
M17-B
B
Jo. B
nocoupl
No.
ibly No
x No.
ipinger
3. A'
-\o.
Lenq
. Tip Dia
e No.
2~
F-K>
B-/
-lookup
/5?/-y
th:_L
o. Mb
Cp-Q.
3158B



Q_ft
in
84_



UH-'H-"


A/V/
:tion (Y) / OIO
jr AH@
% Assumed %CO, /
Train A Pitot Tube Pressure Measurement System Leak Checks
Initial
/^O?

Final
((f\$
^A
Initial


Final


Initial


Final


Initial


Final


Initial


Final


/,n
•?
5 %o2 6


Ct








i
•


r
•




•




• •


LAJ LBJ LcJ LoJ u=J
Traverse Point Layout
)mpass Direction > North
Nozzles are quartz-glass.
Train B Pitot Tube Pressure Measurement System Leak Checks
Initial
/Y37

Final
{tfl'"
ftJ^A
Initial


Final


Initial


Final


Initial


Final


Initial


Final


Train A Sampling System Leak Checks

Time (24 Hr)
Vacuum, in Hg
Leak Rate, cfm
Initial
ltV)
ft
,n4

-------
   Run No.
   Date   f(-f7-M
     Sampling Location  Unit 2A Baahouse Outlet Duct
     Project No.  1 04703.1.002.05.01	
                                                                         Operator.
                                                                         page.
                                                                                    of  2-
                                                   Sampling Data for Method 17 Train A No.   M17-A
    Traverse
     Point
            Sampling
             Time,
              min.
              0
 Clock
 Time
(24-Hr)
        Dry Gas Meter Reading
              (VJ, ft3
        Initial
         Desired
                    Actual
Velocity
 Head
 (Ap),
in. H20
Orifice Pressure
  Differential
    (AH),
   in. H20
                                      Desired  Actual
Stack
Temp.
 
                                                                                                   "7
             '60
             35
                                                                                                   •7
                                                                                                  -7
                                            i?y
                                            /*-
                                                  /.*
                                                          a.
                                             G ,5P
                                                                     ^Z
                                                 13-
                                              g  tf~
             -70
                   an, 9
                                     £12,
                                                 7
             &)
IblG
                                                              -70
                                           , 23-2
                                                                              -7
   Remarks and Notes:
   M17DPQ2.WPD September 1, 1999
26
                                               RCA#2  APPENDIX C

-------
                      40 CFR 60, APPENDIX A, METHOD 3B
                       INTEGRATED GAS SAMPLING DATA
Run No.
                  Date
Project No.  104703.1.002.05.01	
Sample Type (Multi-Point, Single-Point)
Flow Control Device (Valve, Critical Orifice)
Method 5 Meter Box No.	
MSB Pump Type  diaphram
MSB Pump No.    A- ft-
                                        Client/Source U.S. EPA / Cogentrix Unit 2A
                                        Sampling Location Unit 2A Baghouse Outlet
                                        Operator  do'-tf/U	
                                        Bag Type   Tedlar
                                        Method SB Train No._
                                        MSB Flow Meter Type.
                                        MSB Flow Meter No.
                                                              Sample No.
                                                            NA	
                                                                          NA
                                                             rotameter
Desired Sampling Rate
Leak Check Before Sampling
Total Sampling Time     ^
                                  cc/min
Flow Rate, cc/min: Average	
Estimated Total Sample Volume
                              C	  After Sampling
                             min  Average Flow Meter Reading
                            ^/-^	 Highest   '•^e-f	
                                                             Lowest
                                          liters
  Time
 (24-Hr)
         Flow
         Meter
        Reading
                 Start
                 Purge
                          Start
                        Sampling
  Stop
Sampling
Sampling
Remarks and Notes
   IS
 l&i
 frif
        10
M3BSAMP.WPD June 18, 1998
                                                                                    27
                            RCA#2 APPENDIX C

-------
                             40 CFR 60, APPENDIX A, METHOD 3B
                              INTEGRATED GAS SAMPLING DATA
                        Date
Run No.
Project No.  104703.1.002.05.01
Sample Type (Multi-Point, Gingle-Pc
                                      rt)
      Flow Control Device (Valve, Critical Orifice)
      Method 5 Meter Box No.   A)~ll	
      MSB Pump Type   diaohram	
      MSB Pump No.     A^"//	
                       Client/Source U.S. EPA / Cogentrix Unit 2A
                       Sampling Location  Unit 2A Baahouse Outlet
                       Operator   
-------
                                            40 CFR 60, APPENDIX A, METHOD 3B, GAS ANALYSIS BY ORSAT
                        Run No.
n
                                  Date
Project No.  104703.1.002.05.01     Sample No. .
Sampling Location  Unit 2A Baghouse Outlet Duct
Analysis Start Time
                                                                        NA
                        Sample Type (Bag, Grab)
                        Analyst   c/,
                         Bag
Orsat Leak Check Before Analysis:
Burrete   ^o	Change in 4 Minutes
Pipettes  A/o	Change in 4 Minutes
Orsat Leak Check After Analysis:
Burrete   /Sc>     Change in 4 Minutes
Pipettes  A4?     Change in 4 Minutes
Analysis


Gas
C02


02 (Net is actual reading
minus actual C02 reading)

1

Actual
Reading
1 /*/,(*
2 S^lo
3
1 / cf. j cf
2 a A jfr*
r{J*£f
3
Net
Value

/•*.(*


'

2

Actual
Reading
1 /*i4
2 /y&
3
1 tf.P
2 s/:?
3
Net
Value

;#.£•


y,z<

3

Actual
Reading
1
2
3
1
2
3
Net
Value






Average
Net
Value
(% v/v)

S*J-&


4%  0.3% v/v     02   >_15%  0.2% v/v
                                              .<_4%  0.2% v/v          <15%  0.3% v/v
                 Remarks and Notes:
  S3
  co
                 M3BANAL WPD September 3, 1999

-------
  CO
  o
I
KJ
o
                                           40 Cf/7 60. APPENDIX A, METHOD 3B, GAS ANALYSIS BY ORSAT
                       Run No.
                                   Date
Project No.  104703.1.002.05.01     Sample No. .
Sampling Location   Unit 2A Baghouse Outlet Duct
Analysis Start Time .
                                                                       NA
                       Sample Type (Bag, Grab)
                       Analyst
                         Bag
   Orsat Leak Check Before Analysis:
   Burrete   /*£	Change in 4 Minutes
   Pipettes  /y£>	Change in 4 Minutes
   Orsat Leak Check After Analysis:
   Burrete   Wo      Change in 4 Minutes
   Pipettes  yy'o      Change in 4 Minutes
Analysis


Gas
CO2


02 (Net is actual reading
minus actual C02 reading)

1

Actual
Reading
1 /*.?
2 S^,?
3
1 S9.S
2 /$,/
3
Net
Value

;yS
2 S&f
3
1 /9J
2 J$;J
3
Net
Value

s^.$>


"^'

3

Actual
Reading
1
2
3
1
2
3
Net
Value






Average
Net
Value
(% v/v)

/**


T

                                                Acceptance Criteria per Method 3B
                                         CO,
                             0.3% v/v
                             0.2% v/v
0.2% v/v
0.3% v/v
                Remarks and Notes:
                M3BANALWPD September 3, 1999

-------
              40 CFR 60, APPENDIX A, METHOD 17 - PARTICULATE MATTER TRAIN  (M17)
                       FIELD LABORATORY TRAIN SET-UP DATA FOR TWO TRAINS

   MRI Project No. 104703.1.002.05.01
     Client/Source: U.S. EPA OAQPS EMAD EMC / Cogentrix Unit 2A
  Source Location: Rocky Mount, North Carolina
Sampling Location: Baghouse (Fabric Filter) Outlet Duct
  Run No.
Sampling Train A No.
Sampling Train B No..
                      Impinger Box A No.
                      Impinger Box B No..
  Set-up person(s):
Transfer to Sampler:
Relinquished By    «J.
                                          Date:
                  Received By   £>/
                                 Date/Time
      TRAIN COMPONENT
REAGENT
                                                                       LOADING DATA
                                                                           TRAIN A
                                                       TRAIN B
      Sampling Nozzle (Quartz)*

     Filter Assembly and Holder*
                    Filter Type: Whatman QM-A
                Probe (316 SS)
   Sample Transfer/Vacuum Line
 Male 1st Impinger Inlet Blank-Off
                   Nozzle I.D. No.

               Fitter Assembly No.

                 . Filter Holder No.
                                                                             Initial Weights (grams)
         1st Impinger (Mod-GBS) 100-200 mLs ASTM Type I Water
               U-Connector (A)                      •  '•_••
            2nd Impinger (GBS) 100-200 mLs ASTM Type I Water
               U-Connector (B)
         3rd Impinger (Mod-GBS) Empty
               U-Connector (C)
         4th Impinger (Mod-GBS) "200 g indicating silica gel
               U-Connector (D)
         5th Impinger (Mod-GBS) "200 g indicating silica gel
       Impinger Outlet Connector
                Connector I.D. No.
        Before and after sampling: Nozzle inlet opening and filter assembly holder outlet opening covered with Teflon® tape, and
        entire filter assembly holder with filter assembly and nozzle wrapped in aluminum foil and placed in Ziploc® bag. 1st impinger
        inlet sealed with glass blank-off.
Comments:
M17DSUPWPD May 13, 1999 (rev M17DSUP3.WPD November 10, 1999)
                                                                                                       31
                                     RCA#2 APPENDIX C

-------
                  40 CFR 60, APPENDIX A, METHOD 17 - PARTICULATE MATTER TRAIN  (M17)
                       FIELD LABORATORY SAMPLE RECOVERY DATA FOR TWO TRAINS

       MRI Project No. 104703.1.002.05.01
        Client/Source: U.S. EPA OAQPS EMAD EMC / Cogentrix Unit 2A
      Source Location: Rocky Mount, North Carolina
    Sampling Location: Baghouse (Fabric Filter) Outlet Duct
     Run No.
                  Sampling Train A No.
                  Sampling Train B No..
                     Impinger Box A No.     &fsf~T>r>
    Sample recovery person(s):
Weights below are in grams.
Received By
                                                                        Date/Time
                                                                                        Date:
                                             BACK HALF RECOVERIES
                               TRAIN A
 Impinger:     1st
 Final Wt.
 Initial Wt.
   Net Wt.	
Total Condensate Collected:
Description and/or color:
                           2nd
                                   3rd
        4th & 5th
                                                                 1st
                         79.7
                                                 % Blue
                                                                               TRAIN B
2nd
                                                                                  3rd
                                                                           $.3    - ^
                                                                                               4th & 5th
                                                                                               7-7
                                                                                                 $7,3
                                                                                              % Blue
                                            FRONT HALF RECOVERIES
                               TRAIN A
                               102
FILTER ASSEMBLY:
        Sample Number:
   PM Description/color:
TRAIN RINSES:
        Sample Number:  .3V 101
   Components Rinsed*: nozzle, filter holder front
                                                                               TRAIN B
                                                                         103
         *  Acetone rinses with brushing 3 times or more until perceivably clean.

   COMMENTS: Acetone rinses are transferred directly to tared Teflon® beaker liners for analysis.
                                                                                         /
                                                                                  / / lam
   M17DRCV.WPD May 13. 1999 (rev. M17DRCV3.WPD November 10, 1999)
32
                                             RCA#2 APPENDIX C

-------
£
K)
o
                               ft
FIELD SAMPLING DATA FOR METHOD 17 TRAINS
                                                                                                                                              page 1 of
Run No. TI
Date /'(a''
Project No. 104703.
1.002.05.01
Client U.S. EPA OAQPS EMAD EMC
Source Coqentrix Unit 2A
Sampling Locz
Operator fait.
r tfij
Record data e
Barometer No
Barometric Prt
Elevation to IV
Meter Box Pba
Elevation to S
Sampling Loce
Static Pressur
Time (24 Hr)
Pass or Fail

ition Baqhouse Outlet^
/p/v
very A--1)


W^h minutes
Y-20?1
assure
ffrU
in Hg
eter Boxes 34 ft

ampling
ition Pbar
e —2--
70,1$
in Hq
Loc. 34 ft
10 •-!•?
-J^pHg
Train A No. M17-A
Probe No
A
L
Nozzle No. Ml 7-// Tip
Pitot Tube No. A
Stack Thermocouple No.
Filter Holder No. j
Filter Assembly h
Impinger Box No.
Umbilical/Impinge
Umbilical No.
Meter Box No.
DGM Correction
3ngth: _
Cp
10 ft
f% in
0.84

3158A



Jo. F~H
A-
;r Hooki
^
jp UH-
^

/




A' !'2~
Y)
C- yib


Orifice Meter AH(3> /, ?/Y;
•) Pii't-J** /fa (-|2o Assumed
Moisture
I!
Train B No.
Probe No.
Nozzle No..
Pitot Tube Is
Stack Them
Filter Holde
Filter Assen
Impinger Bo
Umbilical/lrr
Umbilical N
Meter Box I
M17-B
B
Lena
MW-fi Tip Dia
•Jo. B
nocoupl
No.
ibly No
x No.
e No. ,
a
/£-/!
B--7
ipinger Hookup
th: 	 1
CP_CL
3158B
i


UH- 2
P_ft
in
3A—




3. A' £•>('" I
•Jo.
"A-''-//
f

DGM Correction (Y) /.- &/f''
Orifice Meter AH@
% Assumed %CO3 _/
Train A Pitot Tube Pressure Measurement System Leak Checks
Initial
fL/i 1 \
L^3/*"V

Final Ini
jt3i<6
rtW>0
I
tial Final



Initial


Final



Initial


Final



Initial


Final



/•/f


^ %o, 5








>


i















LAJ LBJ LcJ LoJ LeJ
Traverse Point Layout
Compass Direction > North
Nozzles are quartz-glass.
Train B Pitot Tube Pressure Measurement System Leak Checks
Initial
oy^o

Final
{Q'ti
Q*i/vrt

Initial


Final



Initial


Final



Initial


Final



Initial


Final




Time (24 Hr)
Vacuum, in Hg
Leak Rate, cfm
Initial
O3i*
\<7
•ooz*
Final Meter Volume
Initial Meter Volume
Leak Check Volume
Final
(Oil
-7
.on"

Initial






Final




Initial






Final




Initial






Final




Initial






Final





Time (24 Hr)
Vacuum, in Hg
Leak Rate, cfm
Initial
OW
h
.*&
Final Meter Volume
Initial Meter Volume
Leak Check Volume
Final
IOM
-7
tQ&

Initial






Final




Initial






Final




Initial



1J.4CI
fcsT, Lit,
M'lH'f
Final



e
Initial



w.w
tH-M
Ht.lli*
Final




   co
   CO
               Remarks and Notes: List any other equipment requiring calibration below.
                                                                                                                             TRAIN A
               M17DPQ1 WPD September 3, 1999
                              Meter Volume at Start of Run


                               Meter Volume at End of Run


                    Total Leak Check or Non-Sample Volume

                                    Adjusted Final Volume

-------
  Run No.
  Date
            Sampling Location  Unit 2A Baahouse Outlet Duct
            Project No.   104703.1.002.05.01	
                                                  Operator  fay.
                                                                  3,/vrl ••>-
                                                                     page.
                                                                                                 of
                                               Sampling Data for Method 17 Train A No.   M17-A
  Traverse
    Point
          Sampling
           Time,
            min.
 0
        Clock
        Time
       (24-Hr)
        Dry Gas Meter Reading
              
*£.
                                                                                        -37
JS.
<2$U-
                                              Z-2.
*
2L
                                                              0-91
                                                           /to
                                                                  yy
                                                                                        -3*5
                                                                             yy
           £-7
                         173,2-0
                                                                                 •35-
                                              0.07
                                           tf.bl
                                                                                    ¥*•
                                                                         3-
                                                                                                   39
                   -£&-
                                                                                            -r
           5V
                                           0-6 t
                                                                                           •7
                                   JL£.
                                                                                            -7
           5*7
                         ISI- 72-
                                                      a-01
                                                          STtf
                                                           53*
       V
                                           6-71
                                                    /#/
                                                                                            "7
                                                                                         3?
           •72-
                                                   0-3-7
                                                   /So
           75
                                                     £1
                                                          7W
             0
                                     Sampling Data for Method 17 Train B No.  M17-B
             •r
                                   ./. 2-
                                                   OSS7
                                                                                                   V/
                                                                                            -7
                                                                                                   ^L
            _/i.
                                               i^=-
                                                               G.I*')
                                                                          Y/
                                                                       (VI
                                                                             ?¥
                                                      a^
                            5, /c
                                                                                         yz.
                            & -f 5"
                                                                                  •7
               3&7V
                                                                                             -7
                                    L2=-
                                                                                                    7-.-?
   Remarks and Notes:
   M17DPG2.WPD Septembers, 1999
34
                                             RCA#2 APPENDIX C

-------
                      40 CFR 60, APPENDIX A, METHOD 3B
                       INTEGRATED GAS SAMPLING DATA
Run No.
         35"
                  Date
Project No.  104703.1.002.05.01 _
Sample Type (Multi-Point, Single-Point)
Flow Control Device (Valve, Critical Orifice)
Method 5 Meter Box No.
MSB Pump Type  diaphram
MSB Pump No.
                       Client/Source U.S. EPA / Cogentrix Unit 2A
                       Sampling Location Unit 2A Baghouse Outlet
                       Operator
                Bag Type  Tedlar
                Method SB Train No._
                MSB Flow Meter Type
                MSB Flow Meter No. _
                                                             Sample No.
                                                            NA _
                                                         NA
                                                             rotameter
Desired Sampling Rate
Leak Check Before  Sampling
Total Sampling Time    ~1D
                                  cc/min
Flow Rate, cc/min: Average	
Estimated Total Sample Volume
              0	  After Sampling
            min  Average Flow Meter Reading
                  	 Highest	
                                                             Lowest
                                          liters
  Time
 (24-Hr)
         Flow
         Meter
        Reading
Start
Purge
  Start
Sampling
  Stop
Sampling
Sampling
Remarks and Notes
        ^L.
 0%
        'b.o
ta£_
M3BSAMP WPD June 18, 1998
                                                                                    35
                           RCA#2 APPENDIX C

-------
  co
  Oi
s
to
fc
*ti
w
o
                                           40 CFR 60, APPENDIX A, METHOD 3B, GAS ANALYSIS BY ORSAT
                       Run No.
                                  Date
Project No.  1Q4703.1.002.05.01     Sample No. .
Sampling Location   Unit 2A Baghouse Outlet Duct
Analysis Start Time _
                                                                       NA
                       Sample Type (Bag, Grab)
                       Analyst    J.
                         Bag
Orsat Leak Check Before Analysis:
Burrete    x^o     Change in 4 Minutes
Pipettes   /*£	Change in 4 Minutes
Orsat Leak Check After Analysis:
Burrete   XV£      Change in 4 Minutes
Pipettes  /*£>	Change in 4 Minutes
Analysis


Gas
C02


02 (Net is actual reading
minus actual CO2 reading)

1

Actual
Reading
1 ss:*
2 /J>,£>
3
1 S&7
2 ;&7
3
Net
Value

SJ»'i?

3,7

2

Actual
Reading
1 s&v
2 s&e
3
1 /eft.?
o y*£ C?
3
Net
Value

/&'O

3.8

3

Actual
Reading
1 AST*
2 /'.5">£
3
21 &- &
Sfji£.j
3
Net
Value

;<5~.o

3,£

Average
Net
Value
(% v/v)

/&,O

x,8

                                               Acceptance Criteria per Method 3B
                                        C02 >4%  0.3% v/v     O2   >:15%   0.2% v/v
                                             <4%  0.2% v/v          <15%   0.3% v/v
                Remarks and Notes:
                M3BANALWPD Septembers, 1999

-------
              40 CFft 60, APPENDIX A,  METHOD 17 - PARTICULATE MATTER TRAIN (M17)
                      FIELD LABORATORY TRAIN SET-UP DATA FOR TWO TRAINS

   MRI Project No.  104703.1.002.05.01
    Client/Source:  U.S. EPA OAQPS EMAD EMC / Cogentrix Unit 2A
  Source Location:  Rocky Mount, North Carolina
Sampling Location:  Baghouse (Fabric Filter) Outlet Duct
  Run No.

  Set-up person(s):
Transfer to Sampler:
Relinquished By
                  Sampling Train A No.
                  Sampling Train B No.
                                    Received By
     TRAIN COMPONENT
                                     REAGENT
                                                           Impinger Box A No.
                                                           Impinger Box B No.
                                                                               Date:
                                                                                       .^
                                                                      Date/Time  JJ/jfW
                                                                       LOADING DATA
                                                                          TRAIN A
                                                                                            TRAIN B
      Sampling Nozzle (Quartz)*

    Filter Assembly and Holder*          .
                   Filter Type: Whatman QM-A
               Probe (31 6 SS)
   Sample Transfer/Vacuum Line
Male 1st Impinger Inlet Blank-Off
                                                        Nozzle I.D. No.

                                                    Filter Assembly No.
                                                    :              .
                                                       Filter Holder No.
        1st Impinger (Mod-GBS) 100-200 mLs ASTM Type I Water
              U-Connector (A)                •''-"...:
           2nd Impinger (GBS) 100-200 mLs ASTM Type :l Water
              U-Connector (B)
        3rd Impinger (Mod-GBS) Empty
              U-Connector (C)
        4th Impinger (Mod-GBS) "200 g indicating silica gel
              U-Connector (D)
        5th Impinger (Mod-GBS) "200 g indicating silica gel
      Impinger Outlet Connector
                                                     Connector I.D. No.
                                                                            Initial Weights (grams)
                                                                               • ~
                                                                                                   ,
                                                                                             / z **f
                                                                               f
                                                                                            '<>"•
       Before and after sampling: Nozzle inlet opening and filter assembly holder outlet opening covered with Teflon® tape, and
       entire filter assembly holder with filter assembly and nozzle wrapped in aluminum foil and placed in Ziploc® bag.  1 st impmger
       inlet sealed with glass blank-off.
Comments:
M17DSUP.WPD May 13, 1999 (rev M17DSUP3.WPD November 10, 1999]
                                                                                                       37
                                     RCA#2 APPENDIX  C

-------
                  40 CFR 60, APPENDIX A, METHOD 17 - PARTICIPATE MATTER TRAIN  (M17)
                       FIELD LABORATORY SAMPLE RECOVERY DATA FOR TWO TRAINS

       MRI Project No. 104703.1.002.05.01
        Client/Source: U.S. EPA OAQPS EMAD  EMC / Cogentrix Unit 2A
      Source Location: Rocky Mount, North Carolina
    Sampling Location: Baghouse (Fabric Filter) Outlet Duct
     Run No.
                  Sampling Train A No.
                  Sampling Train B No.
                                                             Impinger Box A No..
                                                             Impinger Box B No.
Transfer for Recovery:
Relinquished By   Z7,
    Sample recovery person(s):
Weights below are in grams.
                                    C/- £i
                                     Received By
                                                                         Date/Time
                                                                                         Date:
                                             BACK HALF RECOVERIES
                               TRAIN A
                 1st
 Impinger:
  Final Wt.
 Initial Wt.
   Net Wt.	
Total Condensate Collected:
Description and/or color:
                        2nd
3rd
4th & 5th
1st
                                              % Blue
                                                                                TRAIN B
                                                                         2nd
                                                                                   3rd
                                                                                                4th & 5th
                                                                                                  % Blue
                                             FRONT HALF RECOVERIES
                               TRAIN A
   FILTER ASSEMBLY:
           Sample Number: J£5"102
       PM Description/color:   }?)&£>*-	
   TRAIN RINSES:
           Sample Number:  c35""101
       Components Rinsed*: nozzle, filter holder front
                                                                             TRAIN B
         *  Acetone rinses with brushing 3 times or more until perceivably clean.

   COMMENTS: Acetone rinses are transferred directly to tared Teflon® beaker liners for analysis.
   M17DRCV WPD May 13, 1999 (rev. M17DRCV3.WPD November 10, 19991
38
                                             RCA#2 APPENDIX C

-------
n
o
   co
   co
                                                                 FIELD SAMPLING DATA FOR METHOD 17 TRAINS
Run No.
                                   Date
                 Project No.   104703.1.002.05.01
                 Client  U.S. EPA OAOPS EMAD EMC
                 Source  Coaentrix Unit 2A
                 Sampling Location Baahouse Outlet
                 Operator
Record data every A-?
Barometer No.   Y-2021
                                        ' '
                                             minutes
Barometric Pressure   nu<
                    i
Elevation to Meter Boxes
Meter Box Pbar  	ty'
                                            	in Hg
                                            .34	ft
Elevation to Sampling Loc.
Sampling Location Pbar   ^
Static Pressure   ~
                                            	in Hg
                                             34    ft
                               in Hg
                              jn H2O
Train A No. M17-A
Probe No. A Lenath: 10 ft
Nozzle No. M17-p Tic Dia. 0. >Hif in
Pitot Tube No. A CD 0.84
Stack Thermocouple No. 31 58A
Filter Holder No. (e
Filter Assembly No. r n
Impinger Box No. A- /
Umbilical/lmpinqer Hookup UH- 7&
Umbilical No. fU'J&^tf
Meter Box No. A/'^
DGM Correction (Y) d'^%
Orifice Meter AH(5> (fS'lO
Train B No. M17-B
Probe No. B Lenath: 10
Nozzle No. M17-*) Tio Dia. (")rl^
Pitot Tube No. B Cp 0.£
Stack Thermocouple No. 31 588
r—
Filter Holder No. -->
Filter Assembly No. r' '(?>
Impinqer Box No. B- /
Umbilical/lmpinqer Hookup UH- y2
Umbilical No. A/1^?- /
_ft
in
i4_



^~

Meter Box No. /V/7
DGM Correction (Yl / tf/tS
Orifice Meter AH(3> /jBtfa
                                                                                                                                                page 1 of
                                                                                                                           1
                                                      Assumed Moisture
%  Assumed %CO,
                                                                                                                   %O,
       LA]  LfiJ  Lai  LoJ  LEJ
        Traverse Point Layout
   Compass Direction >• North
Nozzles are quartz-glass.

Time (24 Hr)
Pass or Fail
Train A Pitot Tube Pressure Measurement System Leak Checks
Initial
10%

Final
ltf/\
tofiA
Initial


Final


Initial


Final


Initial


Final


Initial


Final


Train B Pitot Tube Pressure Measurement System Leak Checks
Initial
/tilUr

Final
{'2?Jt
rtn&
Initial


Final


Initial


Final


Initial


Final


Initial


Final


                                                                       Train A Sampling System Leak Checks

Time (24 Hr)
Vacuum, in Hg
Leak Rate, cfm
Initial
l"fa
tf
.**>
Final Meter Volume
Initial Meter Volume
Leak Check Volume
Final
M
1
.PCftf

Initial






Final




Initial






Final




Initial






Final




Initial






Final





Time (24 Hr)
Vacuum, in Hg
Leak Rate, cfm
Initial
*#
1$
<6G\
Final Meter Volume
Initial Meter Volume
Leak Check Volume
Final
(Vft
4
.a*

Initial






Final




Initial






Final




Initial



W. Wl
w,w
^"Hi3f)
Final




Initial



u,-w
io,itf
'itf,oi $
Final




                Remarks and Notes:  List any other equipment requiring calibration below.
                                                                                                                               TRAIN A
                                                                                                                                   TRAIN B
                M17DPG1.WPD Septembers, 1999
                                                                               Meter Volume at Start of Run
                                                                                Meter Volume at End of Run
                                                                     Total Leak Check or Non-Sample Volume
                                                                                     Adjusted Final Volume

-------
Run No.
Date
            -36
                    Sampling Location Unit 2A Baohouse Outlet Duct
                    Project No.  104703.1.002.05.01	
                                                                    Operator
                                                                                       page
                                                                                                  of   2.
                                                Sampling Data for Method 17 Train A No.  M17-A
Traverse
  Point
           Sampling
            Time,
             min.
             0
                Clock
                Time
                (24-Hr)
                       Dry Gas Meter Reading
                             (VJ, ft3
                       Initial
                           Desired
                                   Actual
Velocity
 Head
 (Ap),
in. H20
Orifice Pressure
  Differential
    (AH),
   in. H^p
                                                      Desired
                                                           Actual
Stack
Temp.
 (t.).
  °F
Dry Gas Meter
 Temperature
                                                                           Inlet
                                                                                     Outlet
              Pump
             Vacuum
              in. Hg
Silica Gel
Impinger
 Outlet
 Temp.,
   °F
                   f/ffif
                                                           0-&8
                                                                   /ro
                   nu
                   /MY
                       "toi, •%
        0-6-i.
/$0
                                                                                         -7
      I
                a n
                                              0,2.1
                   (\1*
                                                                   r&_
                                                                                           "
                                                                      fgv
                                                                                 &o_
       2.
         •z?
                                                                                ^2,
                                                                                           4=
                   Alb
                                                                   ^L
   ^S.
                   ittL
                                                      0-2*
           &
            71
                       ill-W
                                                              0,60
                                                                             63-
    £-<
                                 &Ul$-
                                                  0-Ti-
                0/?2-
           TT
                                                      6,73
                                 $k
                                                                         63-
                                               0.73
                                                   0,23
                                                                                        •7
            "75
                                                Sampling Data for Method 17 Train B No.  M17-B
                                               73L
                   u&-
                                                                                        JZ.
                                                                                           ^L
                                                      o.-zn
                                                                   /S'Z
                   lllcL
                       ifirfO
                                           ±Z-
             ?
                                                   0-36
                                                                         &L.

            5?
                                                   0.11-
                                                          0''L2
                                                                         £L
                                                                                            -7
                                                      0-12-
                                                                                               *S7
                                                                                            f?
                                                                                    ftf-
                                                                                        ^L
                                                              0MZ-
                                                                             6-7
                                               f,0
                                                                   Mo
                                                                                 65
                                             -7
            70
                          &i
                          W&
                                                "
                                                   o-W
                                                                  i3o_
                               W-
                   (2J*
                                                                                               .£L
   Remarks and Notes:
   M17DPG2.WPD September 3, 1999
40
                                            RCA#2 APPENDIX C

-------
                      40 CFR 60, APPENDIX A, METHOD 3B
                       INTEGRATED GAS SAMPLING DATA
Run No.
                 Date
Project No. 104703.1.002.05.01	
Sample Type  (Multi-Point, Single-Point)
Flow Control  Device (Valve, Critical Orifici
Method 5 Meter Box No.	
MSB Pump Type   diaohram
MSB Pump No.	
                       Client/Source U.S. EPA / Cogentrix Unit 2A
                       Sampling Location Unit 2A Baahouse Outlet
                       Operator
                                       Bag Type  Tedlar
                                       Method SB Train No.
                                       MSB Flow Meter Type
                                       MSB Flow Meter No.
                                                             Sample No.
                                                            NA _
                                                         NA
                                                            rotameter
Desired Sampling Rate	
Leak Check Before Sampling.
Total Sampling Time   "TO
                                  cc/min
Flow Rate, cc/min: Average	
Estimated Total Sample Volume
            <^>	  After Sampling
            min  Average Flow Meter Reading
                  	 Highest	
                                                            Lowest
                                          liters
 Time
 (24-Hr)
         Flow
         Meter
        Reading
Start
Purge
                         Start
                       Sampling
  Stop
Sampling
Sampling
Remarks and Notes
 Hot
 //£/
 HU-
 {&_
  v\o
 ftw
 n-w
M3BSAMP.WPD June 18, 1998
                                                                                    41
                            RCA#2 APPENDIX C

-------
s
to
n
                                           40 CF/? 60, APPENDIX A, METHOD 3B, GAS ANALYSIS BY ORSAT
                       Run No.
                                  Date
Project No.  104703.1.002.05.01     Sample No. .
Sampling Location   Unit 2A Baghouse Outlet Duct
Analysis Start Time .
                                                                       NA
                       Sample Type (Bag, Grab)
                       Analyst   
                         Baa
                Orsat Leak Check Before Analysis:
                Burrete    xVp	Change in 4 Minutes
                Pipettes   /yi>     Change in 4 Minutes
                Orsat Leak Check After Analysis:
                Burrete    /?£     Change in 4 Minutes
                Pipettes  /K?     Change in 4 Minutes
Analysis


Gas
C02


02 (Net is actual reading
minus actual C02 reading)

1

Actual
Reading
1 ;*>.<)
2 J*J ^
3
1 />/.7
2 ;.?
2 J&9
3
1 /tf.7
2y/,7
3
Net
Value

/*>. 9

**

3

Actual
Reading
1 ;w
2 /y,?
3
2 ^,7
3
Net
Value

/y. ^

^/-

Average
Net
Value
(% v/v)

/V.J

*,*

                                               Acceptance Criteria per Method 3B
                                        C02
                             0.3% v/v
                             0.2% v/v
0,
0.2% v/v
0.3% v/v
                Remarks and Notes:
                M3BANALWPD September 3, 1999

-------
              40 CFR 60, APPENDIX A, METHOD 17 - PARTICULATE MATTER TRAIN  (M17)
                       FIELD LABORATORY TRAIN SET-UP DATA FOR TWO TRAINS

   MRI Project No. 104703.1.002.05.01
     Client/Source: U.S. EPA OAQPS EMAD EMC / Cogentrix Unit 2A
  Source Location: Rocky Mount, North Carolina
 Sampling Location: Baghouse (Fabric Filter) Outlet Duct

                                               "9_	  Impinger Box A No.    rj~/	
                                               ?	  Impinger Box B No.     fi')
Run No.   <3&>     Sampling Train A No.
                 Sampling Train B No.
Set-up person(s):    *J> •
                                                                               Date:
Transfer to Sampler:
Relinquished By    cl
                                   Received By  /?,
                                                                      Date/Time  /J/jS]/97
      TRAIN COMPONENT
                                   REAGENT
                                                                       LOADING DATA
      Sampling Nozzle (Quartz)*

     Filter Assembly and Holder*
                   Filter Type: Whatman QM*A
                Probe  (31 6 SS)           :
   Sample Transfer/Vacuum Line            :
 Male 1st Impinger Inlet Blank-Off
                                                      Nozzle I.D. No.

                                                  Fitter Assembly No.
                                                 :     :    •  •
                                                     Filter Holder No.
       1st Impinger (Mod-GBS) 100-200 mLs ASTM Type I Water
             U-Connector (A)
          2nd Impinger (GBS) 100-200 mLs ASTM Type t Water
             U-Connector (B)
       3rd Impinger (Mod-GBS) Empty
             U-Connector (C)
       4th Impinger (Mod-GBS) "200 g indicating silica gel
             U-Connector (D)
       5th Impinger (Mod-GBS) "200 g indicating silica gel
       Impinger Outlet Connector
                                                                         TRAIN A
                                                                                             TRAIN B
                                                                             ~ 9
                                                                            -5
                                                                             Initial Weights (grams)
                                                                          "73"Z?*'2.
                                                   Connector I.D. No.    t>jj-31>
                                                                                            OH -3 A
        Before and after sampling: Nozzle inlet opening and filter assembly holder outlet opening covered with Teflon® tape, and
        entire filter assembly holder with filter assembly and nozzle wrapped in aluminum foil and placed in Ziploc® bag. 1 st impinger
        inlet sealed with glass blank-off.
Comments:
M17DSUP WPO May 13, 1999 (rev. M17DSUP3.WPD November 10, 1999)
                                                                                                       43
                                     RCA#2 APPENDK  C

-------
                  40 CFR 60, APPENDIX A, METHOD  17 - PARTICULATE MATTER TRAIN {Ml 7)
                       FIELD  LABORATORY SAMPLE  RECOVERY DATA FOR TWO TRAINS
       MRI Project No. 104703.1.002.05.01
        Client/Source: U.S. EPA OAQPS EMAD EMC / Cogentrix Unit 2A
      Source Location: Rocky Mount, North Carolina
    Sampling Location: Baghouse (Fabric Filter) Outlet Duct
     Run No.
                  Sampling Train A No.   SWS1?-/?
                  Sampling Train B No. _
Transfer for Recovery:
Relinquished By    P>
  Received By  \J.,
                       Impinger Box A No.   rf'/
                       Impinger Box B No.    &"/
                                                                         Date/Time
    Sample recovery person(s):
Weights below are in grams.
                                   tj, S
                                                   Date:  JtJj})*'.
                                             BACK HALF RECOVERIES
                                TRAIN A
                                                                                TRAIN B
                 1st
 Impinger:
  Final Wt.
 Initial Wt.
   Net Wt.	
Total Condensate Collected:
Description and/or color:
                       2nd
3rd
                                                4th & 5th
                                                              1 st        2nd        3rd      4th & 5th
                                                            •733£
                                                                                                    4 &
                                                 %Blue
                                                                                              % Blue
                                             FRONT HALF. RECOVERIES
                                TRAIN A
                                                                                TRAIN B
FILTER ASSEMBLY:
        Sample Number:  i?£>102
    PM Description/color:    j?)ftJ*-
TRAIN RINSES:
        Sample Number:
                                                                      36, 104
                                                                          103
       Components Rinsed*: nozzle, filter holder front
         *  Acetone rinses with brushing 3 times or more until perceivably clean.

    COMMENTS: Acetone rinses are transferred directly to tared Teflon® beaker liners for analysis.
    M17DRCV.WPD May 13, 1999 Irev. M17DRCV3.WPD November 10. 19991
44
                                             RCA#2 APPENDIX C

-------
                                                                 FIELD SAMPLING DATA FOR METHOD 17 TRAINS
I
n
.   71
Date
                 Run No
                 Project No.   104703.1.002.05.01
                 Client  U.S. EPA OAQPS EMAD EMC
                 Source  Coaentrix Unit 2A _
                 Sampling Location Bauhouse Outlet
                 Operator /an'Tr*-' _
                 Record data every n-'  V'~ ?  minutes
                 Barometer No.  Y-2021 _
Barometric Pressure   "%?/• 2-J
Elevation to Meter Boxes 	
Meter Box Pba,      10,1-0
Elevation to Sampling Loc.
Sampling Location^P,
Static
                                            	in Hg
                                            34	ft
                                            	in Hg
                                             34    ft
- in Hg
. in H2O
Train A No. M17-A
Probe No. A Lenath: 10 ft
Nozzle No. M 17-f^ Tip Dia.rf.fft in
Pitot Tube No. A Cp 0.84
Stack Thermocouple No. 31 58A
Filter Holder No. "7
Filter Assembly No. f~ 1?
Impinaer Box No. A- 2^
Umbilical/lmpinaer Hookup UH- /
Umbilical No. /^^" "/
Meter Box No. /V /2-
DGM Correction (Y) O. fffr
Orifice Meter AH@ /,#/&
Train B No. M17-B
Probe No. B Lenath: 1 0 ft
Nozzle No. M1 7- /"f Tip Dia. ff, f1^^, in
Pitot Tube No. B Cp 0.84
Stack Thermocouole No. 3 1 58B
Filter Holder No. %
Filter Assembly No. r Iff
Impinaer Box No. B- 2—-
Umbilical/lmpinqer Hookup UH- 2^-
Umbilical No. A^So-^/
Meter Box No. /V//
DGM Correction (Y) / - North
Nozzles are quartz-glass.

Time (24 Hr)
Pass or Fail
Train A Pitot Tube Pressure Measurement System Leak Checks
Initial
l
\t>
ton
Final Meter Volume
Initial Meter Volume
Leak Check Volume
Final
QC#h
6
tort

Initial






Final




Initial






Final




Initial






Final




Initial






Final




                Remarks and Notes:  List any other equipment requiring calibration below.
                                                                                           TRAIN A
                                                                    ;i
                M17DPG1 WPD September 3, 1999
                                                            Meter Volume at Start of Run
                                                              Meter Volume at End of Run
                                                   Total Leak Check or Non-Sample Volume
                                                                  Adjusted Final Volume

-------
Run No.
Date __
   •U/ >
Sampling Location . Unit 2A Baohouse Outlet Duct
Project No.  104703.1.002.05.01	
                                                                        Operator.
                                                                                            page.
                                                                                                      of
                  A4
                                                  Sampling Data for Method 17 Train A No.  M17-A
   Traverse
     Point
           Sampling
             Time,
             min.
             a
                 Clock
                 Time
                 (24-Hr)
   Dry Gas Meter Reading
         (VJ, ft3
   Initial
                         Desired
               Actual
Velocity
 Head
 (Ap),
in. H20
 Orifice Pressure
   Differential
     (AH),
    in. H20
Desired  Actual
Stack
Temp.
 (ts),
  °F
Dry Gas Meter
 Temperature
                                                                                  Inlet
                                                                                     Outlet
               Pump
              Vacuum,
               in. Hg
Silica Gel
Impinger
 Outlet
 Temp.,
   °F
                                                                                         ¥7
        Z-
                                                                                                       37
                                                                                                V
     - r
         ffi
                                                         a,
                                                                      5~
       y
         •z.1
             aac^g
                         /77
                                                                                 '¥9
                                                                                             5-
                                                                               7S
            1.1
                                                      An
                                                                       5"
                                                       75
                                                         0,"2-
                    IX GO
                                                 A3
                                                                                     Iff
                                                                          /77
                                                                              52?
                                                                       5-
                                                                                 f?
                                                                                                    •35
                               II
                                                                         122-
            f/
                                                                                                    35
                                                                                 92-
            57
                       0,08
                                                                                                */•
                                                                                                     75
                                           35.
            tf
                                                                     S7&
                                                                       6
            72.
                ye
                                                0,12,
                                                                                             V
                                                  Sampling Data for Method 17 Train B No.  M17-B
                                      ^^
              10
                        •79-11
                                                        &-?#
                            01,10
                                     •LJL.
                        Q-Fn
                 o.-z?
              20
                                                                                                 •r
                                                     0.1 i
                                                                                                 6"
                                                                                         Y?
                                                 0,80
                                                           2,5"
                                                                 0-2.7
                                                                                             5"
             55
                                             OrCf'l
                                0-Z.t
                         /&&
               V?
               -fT
                                                0.F7
                                                         6.2-7
                                                             &-2-1
                                                                               3-7
                                                         OS12-
                                                                                             5"
                                                                               37
                                                 O-CeC
                                                                                         57
                                                                                              5-
                                                                               32.
   Remarks and Notes:
   M17DP62.WPD September 3. 1999
46
                                               RCA#2 APPENDIX C

-------
37  Date
                      40 CFR 60, APPENDIX A, METHOD 3B
                       INTEGRATED GAS SAMPLING DATA
                                to'It
Run No.
Project No.  104703.1.002.05.01	
Sample Type (Multi-Point, Single-Point)
Flow Control Device (Valve, Critical Orifice)
Method 5 Meter Box No.
MSB Pump Type  diaphram
MSB Pump No
                                        Client/Source U.S. EPA / Cogentrix Unit 2A
                                        Sampling Location Unit 2A Baghouse Outlet
                                        Operator _
                                        Bag Type   Tedlar
                                        Method SB Train No._
                                        MSB Flow Meter Type.
                                        MSB Flow Meter No.
                                                 Sample No.
                                                NA	
                                                  NA
                                                rotameter
Desired Sampling Rate .
Leak Check Before Sampling
Total Sampling Time	
                                  cc/min
Flow Rate, cc/min: Average _
Estimated Total Sample Volume
                I	 After Sampling
                min  Average Flow Meter Reading
                    	 Highest	
                                                             Lowest
                                          liters
  Time
 (24-Hr)
         Flow
         Meter
        Reading
    Start
    Purge
  Start
Sampling
  Stop
Sampling
Sampling
Remarks and Notes
         5.0
         1.0
 uc • |
           0
 GO/
                                                          ki-.-.—
M3BSAMPWPD June 18, 1998
                                                                                    47
                            RCA#2 APPENDIX C

-------
 CO
o
                                           40 CFR 60, APPENDIX A, METHOD 3B, GAS ANALYSIS BY ORSAT
                       Run No.
         Date
                       Project No.  104703.1.002.05.01     Sample No. .
                       Sampling Location   Unit 2A Baghouse Outlet Duct
                       Analysis Start Time
                       NA
                       Sample Type (Bag, Grab)
                       Analyst  J, •
Baa
Orsat Leak Check Before Analysis:
Burrete    A*e>     Change in 4 Minutes
Pipettes   jVo     Change in 4 Minutes
Orsat Leak Check After Analysis:
Burrete    Ag	Change in 4 Minutes
Pipettes   A/P     Change in 4 Minutes
Analysis

Gas
C02


O2 (Net is actual reading
minus actual CO2 reading)

1

Actual
Reading
1 S3,*r
2 s^.^
3
1 J9,6>
2 ;9.6>
3
Net
Value

SS'S


&,/

1

Actual
Reading
1 y>5.j>~
2 >;£j>~
3
1 /£^
2 ;9.&
3
Net
Value

S3ji£~


6'J

3

Actual
Reading
1 t3.f
2 ;-jsS~
3
1 Sf-Cr
2 J9.6
3
Net
Value

S3.5~


6.J

Average
Net
Value
(% v/v)

/J?A5~


6J

                                                Acceptance Criteria per Method 3B
                                         C02 >4%  0.3% v/v     02  .£.15%   0.2% v/v
                                             j<4%  0.2% v/v          <15%   0.3% v/v
                Remarks and Notes:
                                                                                                 l/io/11
                M3BANAL WPD September 3, 1999

-------
              40 CFR 60, APPENDIX A, METHOD 17 - PARTICULATE MATTER TRAIN (M17)
                       FIELD LABORATORY TRAIN SET-UP DATA FOR TWO TRAINS

   MRI Project No. 104703.1.002.05.01
     Client/Source: U.S. EPA OAQPS EMAD EMC / Cogentrix Unit 2A
  Source Location: Rocky Mount, North Carolina
Sampling Location: Baghouse (Fabric Filter) Outlet Duct
Run No.
  Set-up person(s):   v>L
Transfer to Sampler:
Relinquished By   J- St
                   Sampling Train A No.
                   Sampling Train B No.
                                                           Impinger Box A No.
                                                           Impinger Box B No..
                                                                               Date:
                                   Received By   47,
                                                                      Date/Time
     TRAIN COMPONENT
                                   REAGENT
                                                                       LOADING DATA
                                                                           TRAIN A
                                                                                           TRAIN B
      Sampling Nozzle (Quartz)*

     Filter Assembly and Holder*
                    Filter Type: Whatman QM-A
                Probe (316 SS)
   Sample Transfer/Vacuum Line
 Male 1st Impinger Inlet Blank-Off
                                                      Nozzle I.D. No.

                                                   Fitter Assembly No.

                                                     Filter Holder No.
         1st Impinger (Mod-GBS) 100-200 mLs ASTM Type I Water
               U-Connector (A)                     ::v
            2nd Impinger (GBS) 100-200 mLs ASTM Type I Water
               U-Connector (B)
         3rd Impinger (Mod-GBS) Empty
               U-Connector (C)
         4th Impinger (Mod-GBS) "200 g indicating silica gel
               U-Connector (D)
         5th Impinger (Mod-GBS) "200 g indicating silica gel
       Impinger Outlet Connector
                                                   Connector I.D. No.
                                                                             Initial Weights (grams)
     *  Before and after sampling: Nozzle inlet opening and filter assembly holder outlet opening covered with Teflon® tape, and
        entire filter assembly holder with filter assembly and nozzle wrapped in aluminum foil and placed in Ziploc® bag. 1 st impinger
        inlet sealed with glass blank-off.
Comments:
M17DSUP.WPD May 13. 1999 Irev M17DSUP3.WPD November 10. 19991
                                                                                                       49
                                     RCA#2 APPENDIX  C

-------
                  40 CFR 60, APPENDIX A, METHOD  17 - PARTICULATE MATTER TRAIN  (M17)
                       FIELD LABORATORY SAMPLE  RECOVERY DATA FOR TWO TRAINS

       MRI Project No. 104703.1.002.05.01
        Client/Source: U.S. EPA OAQPS EMAD EMC / Cogentrix Unit 2A
      Source Location: Rocky Mount, North Carolina
    Sampling Location: Baghouse (Fabric Filter) Outlet Duct
     Run No.
                  Sampling Train A No.
                  Sampling Train B No.
Transfer for Recovery:
Relinquished By   # j
  Received By  cJ. £
                                                             Impinger Box A No.
                                                             Impinger Box B No..
                                                                         Date/Time
        Sample recovery person(s):
   Weights below are in grams.
                                                                                      Date:
                                             BACK HALF RECOVERIES
                                TRAIN A
                                                                                TRAIN B
                 1st
 Impinger:
 Final Wt.
 Initial Wt.
   NetWt.	
Total Condensate Collected:
Description and/or color:
                       2nd
3rd
4th & 5th
                                                                  1st
2nd
                                                                                   3rd
                                                                                                4th & 5th
                                                                                        7.J
                                                                                                  . J
                                                    Blue :
                                             FRONT HALF RECOVERIES
                                                                                               % Blue
                                TRAIN A
                                                                                TRAIN B
    FILTER ASSEMBLY:
           Sample Number:  .57102
       PM Description/color:
    TRAIN RINSES:
           Sample Number:
                                                                   CJ7104
                                                                     .103
   Components Rinsed*: nozzle, filter holder front


     * Acetone rinses with brushing 3 times or more until perceivably clean.

COMMENTS:  Acetone rinses are transferred directly to tared Teflon® beaker liners for analysis.
   M17DRCV.WPD May 13. 1999 (rev. M17DRCV3.WPD November 10. 19991
50
                                             RCA#2 APPENDIX C

-------
                                                                  FIELD SAMPLING DATA FOR METHOD 17 TRAINS
§
to
fc
o
                  Run No.
                                   Date
                  Project No.   104703.1.002.05.01
Client  U.S. EPA OAQPS EMAD EMC
Source  Coaentrix Unit 2A _
Sampling Location Baahouse Outlet
Operator   &r\ flr*^ _
                            minutes
                  Record data every *» ~~ 9 P ''
                  Barometer No.  Y-2021
Barometric Pressure   ^yff
Elevation to Meter Boxes
Meter Box Pbaf       ^/
                                                in Hg
                                              34   ft
Elevation to Sampling Loc.
Sampling Location Pba
              jy
Static Pressure
                                                in Hg
                                              34   ft
                                                in Hg
Train A No. M17-A
Probe No. A Lenath: 1 0 ft
Nozzle No. M17-//0 Tip Dia.  ( ,SlO
Train B No. M17-B
Probe No. B Lenath: 10
Nozzle No. M17-? Tio Dia. ^M>
Pitot Tube No. B Cp 0.8-:
Stack Thermocouple No. 31 58B
Filter Holder No.
Filter Assembly No. f~l^
Impinqer Box No. B- /
Umbilical/lmpinqer Hookup U|H- 32-
Umbilical No. /)/ & " !
_ft
in
L_





Meter Box No. A'//
DGM Correction (Y) /,OIO
Orifice Meter AH@ (- 3 '}£
                                                                                                                                                 page
                                                                                                                                                      1 of  2—
                                                   1
                                     Assumed Moisture
% Assumed %CO2   C)    %O2	£-
       lAj  LBJ  UlJ  UlOEj
        Traverse Point Layout
   Compass Direction >• North
Nozzles are quartz-glass.
<
Time (24 Hr) l
Pass or Fail

Time (24 Hr)
Vacuum, in Hg
Leak Rate, cfm
Train A Pitot Tube Pressure Measurement System Leak Checks
^Initial
ffr
(2ll5
Final
^f
nl^b
\
Initiafjli)
jftfT&lll
P
iQQ3?
Final Meter Volume
Initial Meter Volume
Leak Check Volume

Initial


Final



Final
03£\
•-7




Initial


Final




Initial








Initial

Trair
Final


i A Sam
Final






Initial

pling £
Final


ystem
Initial







Train B Pitot Tube
Initial

<f
Leak C
Final
Oj(£>
f^rz^
hecks
Final




Initial


Pressure Measurement System Leak Checks
Final



Initial







Initial


Final


Initial


Final


Initial Final



Final





Initial









Final





Time (24 Hr)
Vacuum, in Hg
Leak Rate, cfm
Initial^
jp&Cdfl
6
t®n~
Final Meter Volume
Initial Meter Volume
Leak Check Volume
Final
0%
(f
tfffls

Initial






Final




Initial






Final




Initial






Final




Initial






Final




                Remarks and Notes: List any other equipment requiring calibration below.
                                                                                                              TRAIN A
                M17DPG1 WPD September 3, 1999
                                                                                                Meter Volume at Start of Run
                                                                                                 Meter Volume at End of Run
                                                                                      Total Leak Check or Non-Sample Volume
                                                                                                      Adjusted Final Volume

-------
  Run No.
  Date
            Sampling Location Unit 2A Baohouse Outlet Duct
            Project No.  104703.1.002.05.01	
                                                                     page.
                                                                                of.
                                                                    Operator.
                                                Sampling Data for Method 17 Train A No.  M17-A
   Traverse
    Point
           Sampling
            Time,
            min.
             a
        Clock
        Time
       (24-Hr)
       Dry Gas Meter Reading
              
-------
                       40 CFR 60, APPENDIX A, METHOD 3B
                        INTEGRATED GAS SAMPLING DATA
Run No.
                  Date
Project No.  104703.1.002.05.01	
Sample Type (Multi-Point, Single-Point)
Flow Control Device (Valve, Critical Orifi&e)
Method 5 Meter Box No..
MSB Pump Type  diaphram
MSB Pump No.      A//2-
Desired Sampling Rate _
Leak Check Before Sampling.
Total Sampling Time    ~7d>
                Client/Source  U.S. EPA / Coaentrix Unit 2A
                Sampling Location Unit 2A Baahouse Outlet
                Operator.
                Bag Type  Tedlar
                Method SB Train No._
                MSB Flow Meter Type.
                MSB Flow Meter No.
                                                              Sample No.
                                                             NA	
                                                                          NA
                                                              rotameter
                                   cc/min
Flow Rate, cc/min: Average _
Estimated Total Sample Volume
      £>	 After Sampling
      min  Average Flow Meter Reading
          	  Highest __2j!£L__
                                                              Lowest
                                           liters
  Time
 (24-Hr)
         Flow
         Meter
        Reading
                 Start
                 Purge
  Start
Sampling
  Stop
Sampling
Sampling
Remarks and Notes
         3*
         '*•*
M3BSAMP.WPD June 18. 1998
                                                                                    53
                            RCA#2 APPENDIX C

-------
 en
I
K)
o
                                           40 C/7? 60, APPENDIX A, METHOD 3B, GAS ANALYSIS BY ORSAT
                       Run No.
                                  Date
Project No.  104703.1.002.05.01     Sample No. .
Sampling Location   Unit 2A Baghouse Outlet Duct
Analysis Start Time   03J&	
                                                                       NA
                       Sample Type (Bag, Grab)
                       Analyst
                         Baa
Orsat Leak Check Before Analysis:
Burrete ___^£___ Change in 4 Minutes
Pipettes   Srt>     Change in 4 Minutes
Orsat Leak Check After Analysis:
Burrete    />£•>     Change in 4 Minutes
Pipettes   /^t>    Change in 4 Minutes
Analysis


Gas
CO2


O2 (Net is actual reading
minus actual C02 reading)

1

Actual
Reading
1 SJ.6
2 /#>&
3
1 /^7
2 /^7
3
Net
Value

XX «?


c^T/7

2

Actual
Reading
1 S3>0
2 S3,c
3
1 /£7
2 /^/7
3
Net
Value

J3.2


^"7

3

Actual
Reading
1 /3>o
2 /^T/C>
3
1 7/-7
2 xJ/^7
3
Net
Value

J3-0


^?''7

Average
Net
Value
(% v/v)

Jj.ti


&-7

                                                Acceptance Criteria per Method 3B
                                         C02  >4%  0.3% v/v     02   >.15%  0.2% v/v
                                             .<4%  0.2% v/v          < 15%  0.3% v/v
                Remarks and Notes:
                M3BAHALWPD September 3, 1999

-------
              40 CFR 60, APPENDIX A, METHOD 17 - PARTICULATE MATTER TRAIN (M17)
                       FIELD LABORATORY TRAIN SET-UP DATA FOR TWO TRAINS

   MRI Project No. 104703.1.002.05.01
     Client/Source: U.S. EPA OAQPS EMAD EMC / Cogentrix Unit 2A
  Source Location: Rocky Mount, North Carolina
 Sampling Location: Baghouse (Fabric Filter) Outlet Duct
  Run No.
  Set-up person(s):   J.
Transfer to Sampler:
Relinquished By
                   Sampling Train A No.
                   Sampling Train B No.
Impinger Box A No.   r7~/
                                                           Impinger Box B No.    l?'s
                                                                               Date:
                                     Received By  Q,
           Date/Time
      TRAIN COMPONENT
                                     REAGENT
            LOADING DATA
                                                                           TRAIN A
                                                                                            TRAIN B
       Sampling Nozzle (Quartz)*

     Filter Assembly and Holder*
                    Filter Type: Whatman QM-A
                Probe (316 SS)
   Sample Transfer/Vacuum Line
 Male 1st Impinger Inlet Blank-Off
                                                        Nozzle I.D. No.

                                                    Filter Assembly No.

                                                       Filter Holder No,
         1st Impinger (Mod-GBS) 100-200 mLs ASTM Type I Water
               U-Connector (A)                     ;
            2nd Impinger (GBS) 100-200 mLs ASTM Type I Water
               U-Connector (B)
         3rd Impinger (Mod-GBS) Empty
               U-Connector (C)
         4th Impinger (Mod-GBS) "200 g indicating silica gel
               U-Connector (D)
         5th Impinger (Mod-GBS) "200 g indicating silica gel
       Impinger Outlet Connector
                                                     Connector I.D. No.
                                                                             Initial Weights (grams)
        Before and after sampling: Nozzle inlet opening and filter assembly holder outlet opening covered with Teflon® tape, and
        entire filter assembly holder with filter assembly and nozzle wrapped in aluminum foil and placed in Ziploc® bag.  1st impinger
        inlet sealed with glass blank-off.
Comments:
M17DSUP WPD May 13, 1399 (rev. M17DSUP3.WPD November 10, 1999)
                                                                                                       55
                                    RCA#2 APPENDIX C

-------
                 40 CFR 60, APPENDIX A, METHOD 17 - PARTICULATE MATTER TRAIN (M17)
                       FIELD LABORATORY SAMPLE RECOVERY DATA FOR TWO TRAINS
       MRI Project No. 104703.1.002.05.01
        Client/Source: U.S. EPA OAQPS EMAD EMC / Cogentrix Unit 2A
      Source Location: Rocky Mount, North Carolina
    Sampling Location: Baghouse (Fabric Filter) Outlet Duct

                                                    	 Impinger Box A No.    <#•/	
                                                    	 Impinger Box B No.    &'/	
  Run No.  t-ZS"    Sampling Train A No.
                  Sampling Train B No..
Transfer for Recovery:
Relinquished By   iP, Gnri-rfcn	  Received By  «/
     Sample recovery person(s):     J. >
Weights below are in grams.
                                                                        Date/Time
                                                                                                 6330
                                                                                         Date:
                                             BACK HALF RECOVERIES
                               TRAIN A
                                                                             TRAIN B
                 1st
 Impinger:
 Final Wt.
 Initial Wt.
   Net Wt.	
Total Condensate Collected:
Description and/or color:
                       2nd
3rd
4th & 5th
1st
   2nd
LS&3
                                                                                      3rd
                                                                                            4th & 5th
                                                                                                         , 7
                                                               647.3
                                    /7,3
                                                 % Blue
                                                                                              % Blue
                                             FRONT HALF 'RECOVERIES
                               TRAIN A
                                                                             TRAIN B
FILTER ASSEMBLY:
        Sample Number:  ^,fl02
    PM Description/color:
TRAIN RINSES:
        Sample Number:
                                                                     oy-104
       Components Rinsed*: nozzle, filter holder front
         *  Acetone rinses with brushing 3 times or more until perceivably clean.

   COMMENTS: Acetone rinses are transferred directly to tared Teflon® beaker liners for analysis.
   M17DRCV.WPD May 13, 1999 (rev. M17DHCV3.WPD November 10. 1999)
56
                                             RCA#2 APPENDIX C

-------
                                                                  FIELD SAMPLING DATA FOR METHOD 17 TRAINS
o
   en
   —J
                  Run No.
                                   Date
                  Project No.  104703.1.002.05.01
                  Client  U.S. EPA OAQPS EMAD EMC
                  Source  Cogentrix Unit 2A
                  Sampling Location Baghouse Outlet
                  Operator
Record data every f^^i
Barometer No.   Y-2021
                                             minutes
Barometric Pressure   JC'-
Elevation to Meter Boxes
Meter Box Pbar  	3 61
Elevation to Sampling Loc.
Sampling Location Pbar
Static Pressure   '~(k
                           	in Hg
                            34   ft
                                            	in Hg
                                             34    ft
_ in Hg
. in H2O
Train A No. M17-A
Probe No. A Lenath: 1 0 ft
Nozzle No. M1 7-/Y Tio Dia. ^'I'ilf in
Pitot Tube No. A C_ 0.84
Stack Thermocouple No. 3158A
Filter Holder No. 1
Filter Assembly No. r~M
Imoinqer Box No. A- '2-
Umbilical/lmpinaer Hookup UH- /
Umbilical No. /\} /^;
Orifice Meter AH

/, S^tf page 1 of. v 1 Assumed Moisture % Assumed %CO2 TAJ LaJ LoJ LoJ l£j Traverse Point Layout Compass Direction >• North Nozzles are quartz-glass. Time (24 Hr) ' Pass or Fail Train A Pitot Tube Pressure Measurement System Leak Checks Initial »/. .• W* Ifal Final tfcn •rt&> Initial Final Initial Final Initial Final Initial Final Train B Pitot Tube Pressure Measurement System Leak Checks Initial m &*>-& 1 Final c?5/! A)^Xi Initial Final Initial Final Initial Final Initial Final Train A Sampling System Leak CHecks Time (24 Hr) Vacuum, in Hg Leak Rate, cfm Initial^. ^ifytf d3^ ' & .Off Final Meter Volume Initial Meter Volume Leak Check Volume Y 1 Final CKy?*1) ft . o


-------
   Run No.
   Date
                           Sampling Location  Unit 2A Baohouse Outlet Duct
                           Project No.  104703.1.002.05.01  	
                                                                   Operator.
                                                                                           page
                                                                                                     of
                                               Sampling Data for Method 17 Train A No.   M17-A
>/**
   Traverse
    Point
           Sampling
            Time,
            min.
                       Clock
                       Time
                      (24-Hr)
                               Dry Gas Meter Reading
                                     (VJ, ft3
                               Initial
                           Desired     Actual
Velocity
 Head
 (Ap),
in. H20
 Orifice Pressure
  Differential
     (AH),
    in. H20
Desired  Actual
Stack
Temp.
 (ts),
  °F
Dry Gas Meter
 Temperature
                                                                             Inlet
                                                                                       Outlet
              Pump
             Vacuum,
              in. Hg
Silica Gel
Impmger
 Outlet
 Temp.,
   °F
      t
               2
                                                                        777
                                                                                   7*7
                                                                     777
                                                                                                     •5-7
                                             0,20
                                                                                             *1
           l£-
                                                 u^.
                                                                         777
                                                                                           5"
                                                                    Z22_
                                                                                             jfzL
                                                        &,
                                                                     777
                                                                                              A-
           5"?
                                                                        tZL
                                                                                 ZL
                                                                    772-
                                                                               57
                                                                            7*
                                                                    77^
                                                                    777
       2,
                      '3TQI
                                               -o
                                                                    /27_
             0
                                                   Sampling Data for Method 17 Train B No.   M17-B
                                                                                           j£L
                       25^.
                                    (2.5-
                                                                                                     3?
                                                                                          -S
                                                     &.2J3
                 <^T
                                                      0.2$
                                                                         /&>
                                                                                                5"
                              V'/
                                                                                                     ^2L
                                                      o.JI
                                                                                                      -"57
£22.
                                                                C?.Zj?
                                                                                                  '57
                                    f 31.70
                                                                     fT?
                                                 ^'^
                                                          /
                                                                      779
                                                             6-3%
                                                                         fifo
                                                                     Z^L
                                                                                            -
   Remarks and Notes:
                                         >- _    * *     ,o
                                      -  '"  tpf
                                      •
58
                                            RCA#2 APPENDIX C

-------
                      40 CFR 60, APPENDIX A, METHOD 3B
                       INTEGRATED GAS SAMPLING DATA
Run No.
          Date
Project No.  104703.1.002.05.01	
Sample Type (Multi-Point, Single-Point)
Flow Control Device (Valve, Critical Orifice)
Method 5 Meter Box No.	
MSB Pump Type  diaphram
MSB Pump No.    A//2-
                Client/Source U.S. EPA / Coaentrix Unit 2A
                Sampling Location Unit 2A Baghouse Outlet
                Operator
                Bag Type  Tedlar	
                Method SB Train No. _
                MSB Flow Meter Type.
                MSB Flow Meter No. _
                                                             Sample No.
                                                            NA	
                                                                  NA
                                                             rotameter
Desired Sampling Rate	
Leak Check Before Sampling.
Total Sampling Time    *7O
                                  cc/min
Flow Rate, cc/min: Average	
Estimated Total Sample Volume
                                      After Sampling
                     min  Average Flow Meter Reading
                               Highest
                                                             Lowest ^**&
                        7!
                                          liters
 Time
 (24-Hr)
 Flow
 Meter
Reading
                 Start
                 Purge
  Start
Sampling
  Stop
Sampling
Sampling
Remarks and Notes
         3,0
 dfol-
        $.0
 anon
 ofot
         10
M3BSAMPWPD June 18, 1998
                                                                                    59
                            RCA#2 APPENDIX C

-------
1
o
                                          40 C/7? 60, APPENDIX A, METHOD 3B, GAS ANALYSIS BY ORSAT
                      Run No.
                                  Date
Project No.  104703.1.002.05.01     Sample No. .
Sampling Location   Unit 2A Baghouse Outlet Duct
Analysis Start Time
                                                                      NA
                      Sample Type (Bag, Grab)
                      Analyst   j


^T^>

3

Actual
Reading
1 S33
2 J-3,3
3
1 W.t,
2 ;$-,&•
3
Net
Value
J33



&,?

Average
Net
Value
(% v/v)
;33


2


                                               Acceptance Criteria per Method 3B
                                        CO,
                             0.3% v/v
                             0.2% v/v
0,
0.2% v/v
0.3% v/v
               Remarks and Notes:
               M3BANAL.WPD September 3. 1999

-------
               40 CFR 60, APPENDIX A, METHOD 17 - PARTICULATE MATTER TRAIN (M17)
                       FIELD LABORATORY TRAIN SET-UP DATA FOR TWO TRAINS

    MRI Project No. 104703.1.002.05.01
     Client/Source: U.S. EPA OAQPS EMAD EMC / Cogentrix Unit 2A
   Source Location: Rocky Mount, North Carolina
 Sampling Location: Baghouse (Fabric Filter) Outlet Duct
  Run No.   &s    Sampling Train A No.   /$?SJ?-/9	  Impinger Box A No.
                   Sampling Train B No.   ^V 7 &	  Impinger Box B No.
                                                 _
   Set-up person(s):    J • $usy?r3s~r _   Date:
Transfer to Sampler:
Relinquished By   J- Stjx^^^^-ry      Received By  &. &^-jf^~J r?       Date/Time _/J//9/9<3'
                                                                                      ^
      TRAIN COMPONENT __ REAGENT __ LOADING DATA

                                                                           TRAIN A          TRAIN B

       Sampling Nozzle (Quartz)*                 .          Nozzle I. D. No.  /"J&-

     Filter Assembly and Holder*                    ...  Fitter Assembly No. _ /_2
                    Filter Type: Whatman QM-A     '."'-'
                Probe (31 6 SS)                          Filter Holder No,       <3 _      ^
    Sample Transfer/Vacuum Line                . .
 Male 1st Impinger Inlet Blank-Off                     .   .:
                                                                             Initial Weights (grams)
         1st Impinger (Mod-GBS) 100-200 mLs ASTM Type I Water
               U-Connector (A)
             2nd Impinger (GBS) 100-200 mLs ASTM Type I Water
               U-Connector (B)
         3rd Impinger (Mod-GBS) Empty
               U-Connector (C)
         4th Impinger (Mod-GBS) "200 g indicating silica gel
               U-Connector (D)
         5th Impinger (Mod-GBS) "200 g indicating silica gel

       Impinger Outlet Connector                        Connector I.D. No.     UH -)
        Before and after sampling: Nozzle inlet opening and filter assembly holder outlet opening covered with Teflon® tape, and
        entire filter assembly holder with filter assembly and nozzle wrapped in aluminum foil and placed in Ziploc® bag.  1 st impinger
        inlet sealed with glass blank-off.
Comments:
M17DSUP WPD May 13, 1999 {rev M17DSUP3 WPD November 10. 1999)
                                                                                                       61
                                     RCA#2 APPENDIX C

-------
                  40 CFR 60, APPENDIX A, METHOD 17 - PARTICULATE MATTER TRAIN (M17)
                       FIELD LABORATORY SAMPLE RECOVERY DATA FOR TWO TRAINS
       MRI Project No. 104703.1.002.05.01
        Client/Source: U.S. EPA OAQPS EMAD EMC / Cogentrix Unit 2A
      Source Location: Rocky Mount, North Carolina
    Sampling Location: Baghouse (Fabric Filter) Outlet Duct
                                                             Impinger Box A No.    /#'**
                                                             Impinger Box B No.     &'&•
  Run No.  39    Sampling Train A No.
                  Sampling Train B No.
Transfer for Recovery:
Relinquished By    47 fenfJ-Jn	 Received By   J, £usjtr>'2s->       Date/Time
    Sample recovery person(s): 	d, Sujfj?? &.si	
Weights below are in grams.
 	BACK HALF RECOVERIES	
                               TRAIN A
 Impinger:     1st
  Final Wt.
 Initial Wt.
   Net Wt.	
Total Condensate Collected:
Description and/or color:
                           2nd
                          1*9*3
                                   3rd
4th & 5th
   1st
L^.L

                                                 % Blue
                                                                                TRAIN B
  2nd
723 sj
                                                                                   3rd
                                                                                       0
                                                 4th & 5th
                                                                                               % Blue
                                             FRONT 'HALF RECOVERIES
                               TRAIN A
                                                                             TRAIN B
FILTER ASSEMBLY:
        Sample Number:  >59 102
    PM Description/color:
TRAIN RINSES:
        Sample Number:
   Components Rinsed*: nozzle, filter holder front
                                                                      ^5104
                                                                          103
         *  Acetone rinses with brushing 3 times or more until perceivably clean.

   COMMENTS: Acetone rinses are transferred directly to tared Teflon® beaker liners for analysis.
   M17DRCV.WPD May 13, 1999 (rev. M17DRCV3.WPD November 10. 19991
62
                                             RCA#2 APPENDIX  C

-------
                                                                FIELD SAMPLING DATA FOR METHOD 17 TRAINS
                Run No.   'TO     Date  Ij'^'^l
                Project No.  104703.1.002.05.01
                Client  U.S. EPA OAQPS EMAD EMC
                Source  Cogentrix Unit 2A	
                Sampling Location Baahouse Outlet
                Operator    ^u^-~~~	
                Record data every A'? \>- s minutes
                Barometer No.  Y-2021	
                Barometric Pressure 	t
                Elevation to Meter Boxes
                Meter Box Pbar 	/:
	in Hg
 34    ft
               Elevation to Sampling Loc.
               Sampling Location P
               Static Pressure
	in Hg
 34    ft
   . in Hg
Train A No. M17-A
Probe No. A Length: 10 ft
Nozzle No. M17-? Tio Dia. O-M \n
Pilot Tube No. A C 0.84
Stack Thermocouple No. 3158A
Filter Holder No. ?
Filter Assembly No. /"2-f
Impinger Box No. A- f
Umbilical/lmpinqer Hookup UH- ")°
Umbilical No. N^O-i
Meter Box No. /V i V-
DGM Correction (Yi ffr6^^
Orifice Meter AH<5> {'8l&
TrainB No. M17-B
Probe No. B Length: 10
ft
Nozzle No. M 17- /OTip Dia.£>"' $ in
Pilot Tube No. B C, 0.84
Stack Thermocouple No. 31 58B
Filter Holder No. £>•
Filter Assemblv No. f^H^
Impinqer Box No. B- /
Umbilical/lmpinger Hookup UH- ~3~l —
Umbilical No. A/ ^O - /






Meter Box No. A/ ll
DGM Correction M (rOl&
Orifice Meter AH@ /.%°)%
                                                                                                                                              page 1 of



•
>
•



• • • •
f
1 • • • •
          Assumed Moisture
                                                                                          Assumed %CO2.
                             %02
            Laf uu  LnJ  L£J
        Traverse Point Layout
   Compass Direction > North
Nozzles are quartz-glass.

Time (24 Hr)
Pass or Fail

Train A Pitot Tube Pressure Measurement System Leak Checks
Initial
QffH

Final
(Ol'l'
U&&P
\
Initial


Final



Initial


Final



Initial

Train
Final


Initial


Final


A Sampling System
Train B Pitot Tube Pressure Measurement System Leak Checks
Initial
C/frf3
Leak C
Final
/tiff'
too^
iecks
Initial


Final



Initial


Final



Initial


Final



Initial


Final



a
o

Time (24 Hr)
Vacuum, in Hg
Leak Rate, cfm
Initial
o?,Hl
1^
,0IV
Final Meter Volume
Initial Meter Volume
Leak Check Volume
Final
(GVl
(f
/'Of

Initial






Final




Initial






Final




Initial






Final




Initial






Final





Time (24 Hr)
Vacuum, in Hg
Leak Rate, cfm
Initial
(W
-------
       Run No.
       Date
                  Sampling Location  Unit 2A Baohouse Outlet Duct
                  Project No.  104703.1.002.05.01	
                                                                Operator.
                                                                                    page
                                                                                               of
                                                      Sampling Data for Method 17 Train A No.   M17-A
               Sampling
                Time,
Traverse
  Point
                 min.
                 0
              Clock
              Time
              (24-Hr)
                    Dry Gas Meter Reading
                           (Vm), ft3
                    Initial
                      Desired
                                Actual
Velocity
 Head
 (Ap),
in. H20
         Orifice Pressure
           Differential
             (AH),
            in. H20
        Desired  Actual
Stack
Temp.
 It.).
  °F
Dry Gas Meter
 Temperature
Inlet    Outlet
               Pump
              Vacuum,
               in. Hg
Silica Gel
Impinger
 Outlet
 Temp.,
   °F
                                                                     0-53
                        tffoi
                                                    &ZL
                                                                                                 3£L
                                                                                    6&-
                                                            ffrT),
                '-4-
                                                    &&.
                -V
                                                                     a •
          -*-
                              4^
                                                                     #
                                                                  S&L.
                                                                                  U:-
                                                                     6,1-1
                                                                           (
                                                                                     IY
                                                     0.72-
                                                             O.'Z-'T-
                                                                             7^
                        Iff 0(1
                                                                     0-2-5
                                                                   JK
                                                                                                             V-7
                        SOlO
                                             -
                                                     A -7"!
                                                     2$"
                               h  -
                                     3b
-------
                      40 CFR 60, APPENDIX A, METHOD 3B
                       INTEGRATED GAS SAMPLING DATA
Run No.
          Date
Project No.  104703.1.002.05.01
Sample Type (Multi-Point, Single-Point)
Flow Control Device (Valve, Critical Orifice)
Method 5 Meter Box No.
MSB Pump Type  diaphram
MSB Pump No.	/Vf2-
                       Client/Source U.S. EPA / Coaentrix Unit 2A
                       Sampling Location  Unit 2A Baahouse Outlet
                       Operator.
                Bag Type  Tedlar
                Method SB Train No._
                MSB Flow Meter Type.
                MSB Flow Meter No.
                                                      Sample No.
                                                     NA	
                                                         NA
                                                     rotameter
Desired Sampling Rate
Leak Check Before Sampling.
Total Sampling Time
                           cc/min
Flow Rate, cc/min: Average
Estimated Total Sample Volume
             • (?	 After Sampling
            min  Average Flow Meter Reading
               	 Highest _
                                                     Lowest
                                   liters
  Time
 (24-Hr)
 Flow
 Meter
Reading
Start
Purge
  Start
Sampling
  Stop
Sampling
Sampling
Remarks and Notes
 09 if
 erftf
 oft.
          v
         1*0
         •to
M3BSAMP WPD June 18, 1998
                                                                                    65
                            RCA#2 APPENDIX C

-------
I
KJ
m
o
                                          40 CFR 60, APPENDIX A. METHOD 3B, GAS ANALYSIS BY ORSAT
                      Run No.
                                  Date
Project No.  104703.1.002.05.01     Sample No. .
Sampling Location   Unit 2A Baghouse Outlet Duct
Analysis Start Time .
                                                                      NA
                      Sample Type (Bag, Grab)
                      Analyst    J.
                         Baa
                             Orsat Leak Check Before Analysis:
                             Burrete   A^     Change in 4 Minutes
                             Pipettes  Ab	Change in 4 Minutes
                             Orsat Leak Check After Analysis:
                             Burrete   /Vp	Change in 4 Minutes
                             Pipettes  M>	Change in 4 Minutes
Analysis


Gas
CO2


O2 (Net is actual reading
minus actual C02 reading)

1

Actual
Reading
1 S&.&"
2 /£££"
3
1 ;&?
2 Jfr JP*
3
Net
Value
^,
;&.&


&.3

2

Actual
Reading
1 sao-
2 S&sT'
3
1/tk fa*
/\J tO
2 jJr fr
3
Net
Value

;#.£>


6.3

3

Actual
Reading
1 ^2£-
2 jX.g'
3
1 s*.r
2 jJ^ P*
3
Net
Value

/^7-cS-


£,.3

Average
Net
Value
(% v/v)

S&'V


4, ,3

                                               Acceptance Criteria per Method 3B
C02
0.3% v/v
0.2% v/v
                                          02
                                              <15%
                                                                             0.2% v/v
                                                                             0.3% v/v
               Remarks and Notes:
               M3BANAL.WPD September 3, 1999

-------
              40 CFR 60, APPENDIX A, METHOD 17 - PARTICULATE MATTER TRAIN  (M17)
                       FIELD LABORATORY TRAIN SET-UP DATA FOR TWO TRAINS

   MRI Project No. 104703.1.002.05.01
     Client/Source: U.S. EPA OAQPS EMAD EMC / Cogentrix Unit 2A
   Source Location: Rocky Mount, North Carolina
 Sampling Location: Baghouse (Fabric Filter) Outlet Duct
  Run No.  #0    Sampling Train A No.
                   Sampling Train B No.
  Set-up person(s):    J,
                       Impinger Box A No.
                       Impinger Box B No..
                                          /7~/
                                          Date:
Transfer to Sampler:
Relinquished By     
Received By   O>£SJT>> *
                                 Date/Time
      TRAIN COMPONENT
REAGENT
                                  LOADING DATA
                                                                           TRAIN A
                                                                                            TRAIN B
       Sampling Nozzle (Quartz)*

     Filter Assembly and Holder*
                    Filter Type: Whatman QM-A,
                Probe (316 SS)
    Sample Transfer/Vacuum Line
 Male 1st Impinger Inlet Blank-Off
             j      Nozzle I.D. No.

             I'.. Filter Assembly No.

             ;     Filter Holder No-
                                                                            Initial Weights (grams)
         1st Impinger (Mod-GBS) 100-200 mLs ASTM Type I Water
               U-Connector (A)                     ;    .
            2nd Impinger (GBS) 100-200 mLs ASTM Type I Water
               U-Connector (B)
         3rd Impinger (Mod-GBS) Empty
               U-Connector (C)
         4th Impinger (Mod-GBS) "200 g indicating silica gel
               U-Connector (D)
         5th Impinger (Mod-GBS) "200 g indicating silica gel
                                           . -3
       Impinger Outlet Connector
                Connector I.D. No.
     *  Before and after sampling: Nozzle inlet opening and filter assembly holder outlet opening covered with Teflon® tape, and
        entire filter assembly holder with filter assembly and nozzle wrapped in aluminum foil and placed in Ziploc® bag.  1 st impinger
        inlet sealed with glass blank-off.
Comments:
M17DSUP WPD May 13. 1999 (rev. M17DSUP3 WPD November 10, 19991
                                                                                                       67
                                     RCA#2 APPENDIX C

-------
                  40 CFR 60, APPENDIX A, METHOD 17 - PARTICULATE MATTER TRAIN (Ml7)
                       FIELD LABORATORY SAMPLE RECOVERY DATA FOR TWO TRAINS
       MRI Project No. 104703.1.002.05.01
        Client/Source: U.S. EPA OAQPS EMAD EMC / Cogentrix Unit 2A
      Source Location: Rocky Mount, North Carolina
    Sampling Location: Baghouse (Fabric Filter) Outlet Duct
     Run No.
                  Sampling Train A No.
                  Sampling Train B No.
Impinger Box A No.
Impinger Box B No..
                                                                                  &'}
Transfer for Recovery:
Relinquished By   D> &*•;•£+'n	  Received By
    Sample recovery person(s):      J.
Weights below are in grams.
                                                                         Date/Time
                                                                                          Date-
                                             BACK HALF RECOVERIES
                                TRAIN A
                                                                                 TRAIN B
Impinger:     1st
Final Wt.  (#^£$
Initial Wt.  -£~96.t>
 Net Wt.
                           2nd
                                   3rd
                                                4th & 5th
                                              *?£>?, 1+7t>K~}
                                                              1st
               2nd
                                                                                    3rd
                                   4th & 5th
                                                                                                      . -7
                                                                                                   y.9
    Total Condensate Collected:
    Description and/or color:
                                                  % Blue
                                             FRONT HALF RECOVERIES
                                                                                               % Blue
                                TRAIN A
                                                                                 TRAIN B
    FILTER ASSEMBLY:
           Sample Number:   ^#102
       PM Description/color:
    TRAIN RINSES:
           Sample Number:
       Components Rinsed*: nozzle, filter holder front


         *  Acetone rinses with brushing 3 times or more until perceivably clean.

    COMMENTS: Acetone rinses are transferred directly to tared Teflon® beaker liners for analysis.
   M17DRCV.WPD May 13. 1999 (rev M17DRCV3.WPD November 10, 19991
68
                                              RCA#2 APPENDIX C

-------
                                                                 FIELD SAMPLING DATA FOR METHOD 17 TRAINS

                Run No.
                                  Date
                Project No.  104703.1.002.05.01
                Client  U.S. EPA OAQPS EMAD EMC
                Source  Cogenlrix Unil 2A
                Sampling Localion Baohouse Outlet
                Qperalor
Record dala every A'*?
Barometer No.   Y-2021
                                            minutes
Baromelric Pressure   Qu
Elevalion lo Meier Boxes
Meier Box Pbar     ^O'C^
                                           _ in Hg
                                            34    ft
                                           	in Hg
                                            34    fl
Elevalion lo Sampling Loc.
Sampling Localion Pbar   "¥)' Ol  in Hg
Static PressureM"ZffJ~  •')«••'    in H2O  Assumed Moisture
Train A No. M17-A
Probe No. A Length: 1 0 ft
Nozzle No. Miy-te Tin Dia. (W/b in
Pilot Tube No. A Cp 0.84
Stack Thermocouple No. 31 58A
Filler Holder No. "7
Filler Assembly No. r^b
Impinqer Box No. A- £-
Umbilical/lmpinger Hookup UH- ^
Umbilical No. (0 ty'^
Meier Box No. & /2-
DGM Correclion (Y) & 'Fffi
Orifice Meier AH@ ('#{0
Train B No. M17-B
Probe No. B f Lenalh: 10 fl
Nozzle No. M1 7-'^.J:ip Dia. ^V^ in
r-1
Pilol Tube No. B C 0.84
Stack Thermocouple No. 3158B
Filler Holder No. %F
Filler Assemblv No. f*2jtf
Impinqer Box No. B-^£-
Umbilical/lmpinqer Hookup UH- ^*'"~
Umbilical No. p^"!
Meter Box No. /V / 1
DGM Correction (Y) S'O(&
Orifice Meter AH@ //• &?&'
                                                                                                                                               page 1 of.
                                                                                                                       •  5  •
                                                                                                                          Y
                                                                                                                       •  1
                                                                                        %  Assumed %CO2   (<7     %O2
                                                                                                                      TAJ  LBJ  LcJ  LnJ  L£J
                                                                                                                        Traverse Point Layout
                                                                                                                   Compass Direction > North
                                                                                                               Nozzles are quartz-glass.

Time (24 Hr)
Pass or Fail
Train A Pilot Tube Pressure Measurement System Leak Checks
Initial
tttff

Final
llM
wnA
Initial


Final


Initial


Final


Initial


Final


Initial


Final


Train B Pilot Tube Pressure Measurement System Leak Checks
Initial
(tfft

Final
frW
OC
Final Meier Volume
Initial Meier Volume
Leak Check Volume
ti
Final
W\o
7
b
-------
     Run No.
     Date
                            Sampling Location Unit 2A Baahouse Outlet Duct
                            Project No.  104703.1.002.05.01	
                                                                     Operator
                                                                                page,
                                                                                          of
                                                 Sampling Data for Method 17 Train A No.   M17-A
.//•IT
     Traverse
       Point
             Sampling
              Time,
               min.
                        Clock
                        Time
                       (24-Hr)
                    Dry Gas Meter Reading
                          (VJ, ft3
                    Initial
                             Desired    Actual
Velocity
 Head
 (Ap),
in. H20
Orifice Pressure
  Differential
    (AH),
   in. H;0
                                               Desired  Actual
                                                               Stack
                                                               Temp.
Dry Gas Meter
 Temperature
    (tj,
     °F
                                                                               Inlet
                                                                                       Outlet
 Pump
Vacuum,
 in. Hg
                                                                                     tt-
                                               £3-
                                                                        &L
                                                                                   JL
                -t
                                                                                     xV
                                                                      /&/
                                                                         Sf&
                                                                             -77

                                                                             2Z_
                               , 7!
                                                                       ffe-
                                                                                XSL
                                                                              9*
                                                                                     77
                                                                                              C,
                                                                                     -77
                                                                      ZZfL
                                                                                           3-5"
^J

                                                                        &%-
                                                                              yz.
                                                                             !?*>
                                                                                      7*5
         z.
                                     725.26
                                                         0-17
                                                                            •77
\L\le
                                                       a.&r
                                                                              •5*3
                                                                                            7
                                                ZT
                                                                         /22_
                                                 Sampling Data for Method 17 Train B No.   M17-B
                                                10
                                                                              ^_
             25
                    Affe
                                                                                              JSL
              35
                                                                        ^^:
                                                                     :S.
                           Wl&
                                                                                       33-
                    (ICZ.
                             /ftf'F0
                                                                                ft
              55"
                                                  ZiC
                    fUi-
                                                ^^^
                                                                                            s~
                    £^_
                                     Zfg,
                                                                 a^/7
                                                                            ^-
                                            J7_
     Remarks and Notes:

              "(3 ^/^
     M17DPQ2.WPD September 3. 1999
  70
                                             RCA#2 APPENDIX C

-------
                      40 CFR 60, APPENDIX A, METHOD 3B
                       INTEGRATED GAS SAMPLING DATA
Run No.
          T/
                 Date
Project No.  104703.1.002.05.01	
Sample Type (Multi-Point, Single-Point)
Flow Control Device (Valve, Critical Orific
Method 5 Meter Box No..
MSB Pump Type  diaphram
MSB Pump No.	
                Client/Source U.S. EPA / Coaentrix Unit 2A
                Sampling Location Unit 2A Baahouse Outlet
                Operator
                Bag Type  Tedlar
                Method 3B Train No. _
                MSB Flow Meter Type
                MSB Flow Meter No. _
                                                             Sample No.
                                                            NA _
                                                                          NA
                                                             rotameter
Desired Sampling Rate _
Leak Check Before Sampling.
Total Sampling Time    ^2?
                                  cc/min
Flow Rate, cc/min: Average	
Estimated Total Sample Volume
                            \	  After Sampling
                             min  Average Flow Meter Reading
                                   	 Highest _
                                                             Lowest
                                          liters
 Time
 (24-Hr)
         Flow
         Meter
        Reading
                 Start
                 Purge
  Start
Sampling
  Stop
Sampling
Sampling
Remarks and Notes
        10
 mi
         *>.
-------
s
n
                                          40 C/7? 60, APPENDIX A, METHOD 3B. GAS ANALYSIS BY ORSAT
                      Run No.
                                  Date
Project No.  104703.1.002.05.01     Sample No. .
Sampling Location   Unit 2A Baghouse Outlet Duct
Analysis Start Time
                                                                      NA
                      Sample Type (Bag, Grab)
                      Analyst     J.
                         Bag
Orsat Leak Check Before Analysis:
Burrete    Ai>     Change in 4 Minutes
Pipettes   /fo     Change in 4 Minutes
Orsat Leak Check After Analysis:
Burrete    //£>    Change in 4 Minutes
Pipettes   A^D     Change in 4 Minutes
Analysis


Gas
C02


O2 (Net is actual reading
minus actual CO2 reading)

1

Actual
Reading
1 /2-£
2 J3.Z
3
2 Jfy2^
3
Net
Value

/J/

£-.9

2

Actual
Reading
1 #3
2 /J>3
3
1 ;?.z-
3
Net
Value

//•
M
.479

3

Actual
Reading
1 &3
2 /3,3
3
2 /0.Z-
3
Net
Value

/*->-'

*'^

Average
Net
Value
(% v/v)



«?

                                        CO,
                        Acceptance Criteria per Method 3B
                          .   0.3% v/v     02  ^.15%   0.2% v/v
                          .   0.2% v/v         <15%   0.3% v/v
               Remarks and Notes:
               M3BANALWPD Septembef 3. 1999

-------
               40 CFR 60, APPENDIX A, METHOD 17 - PARTICULATE MATTER TRAIN (M17)
                       FIELD LABORATORY TRAIN SET-UP DATA FOR TWO TRAINS

    MRI Project No.  104703.1.002.05.01
     Client/Source:  U.S. EPA OAQPS EMAD EMC / Cogentrix Unit 2A
   Source Location:  Rocky Mount, North Carolina
 Sampling Location:  Baghouse (Fabric Filter) Outlet Duct
Run No.
                   Sampling Train A No.
                   Sampling Train B No.
   Set-up person(s):
 Transfer to Sampler:
 Relinquished By
                                                          Impinger Box A No.
                                                          Impinger Box B No. .
                                                                             Date:
      TRAIN COMPONENT
Received By  O> &JTJ/-/>>»

REAGENT	
                                                                    Date/Time
                                                                        LOADING DATA
                                                                           TRAIN A
                                                                                           TRAIN B
       Sampling Nozzle (Quartz)*

      Filter Assembly and Holder*
                    Filter Type:  Whatman QM-A
                 Probe (316 SS)           :
    Sample Transfer/Vacuum Line           :.
 Male 1st Impinger Inlet Blank-Off
                                                      Nozzle I.D. No.

                                                  Fitter Assembly No.

                                                     Filter Holder No,
                                                                             Initial Weights (grams)
         1st Impinger (Mod-GBS)  100-200 mLs ASTM Type I Water
                U-Connector (A)                      j.
             2nd Impinger (GBS)  100-200 mLs ASTM Tyjje 1 Water
                U-Connector (B)
         3rd Impinger (Mod-GBS)  Empty
                U-Connector (C)
         4th Impinger (Mod-GBS)  "200 g indicating silica gel
                U-Connector (D)
         5th Impinger (Mod-GBS)  "200 g indicating silica gel
       Impinger Outlet Connector
                                                   Connector I.D. No.
      *  Before and after sampling: Nozzle inlet opening and filter assembly holder outlet opening covered with Teflon® tape, and
        entire filter assembly holder with filter assembly and nozzle wrapped in aluminum foil and placed in Ziploc® bag. 1st impinger
        inlet sealed with glass blank-off.
Comments:
M17DSUP.WPD May 13. 1999 Irev. M17DSUP3.WPD November 10, 19991
                                                                                                       73
                                     RCA#2 APPENDIX C

-------
                  40 CFR 60, APPENDIX A, METHOD 17 - PARTICULATE MATTER TRAIN (M17)
                       FIELD LABORATORY SAMPLE RECOVERY DATA FOR TWO TRAINS
       MRI Project No. 104703.1.002.05.01
        Client/Source: U.S. EPA OAQPS EMAD EMC / Cogentrix Unit 2A
      Source Location: Rocky Mount, North Carolina
    Sampling Location: Baghouse (Fabric Filter) Outlet Duct
  Run No.
                      Sampling Train A No.
                      Sampling Train B No.
                                                          Impinger Box A No.
                                                          Impinger Box B No.
Transfer for Recovery:
Relinquished By   ft,
                                        Received By
                                   Date/Time
    Sample recovery person(s):
Weights below are in grams.
                                    
-------
                                                                FIELD SAMPLING DATA FOR METHOD 17 TRAINS
s
K>
fc
"•d
tn
n
                Run No.
                  Date
                Project No.  104703.1.002.05.01
                Client  U.S. EPA OAQPS EMAD EMC
                Source  Coaentrix Unit 2A
                Sampling Location Baghouse Outlet
                Operator
Record data every A*
Barometer No.  Y-2021
                                       **) minutes
                                              in Hg
                                           34    ft
Barometric Pressure
Elevation to Meter Boxes  _
Meter Box Pba,     '2AtC{i
Elevation to Sampling Loc.
Sampling Location Pbaf  "xV' '3  in Hg
              /ffl*2£f"  if-t>7
Static Pressure y^f^ " '••"    in H2O  Assumed Moisture
                                          	in Hg
                                           34    ft
Train A No. M17-A
Probe No. A Lenath: 10 ft
Nozzle No. M17- °j Tio Dia. ^Hlf in
Pitot Tube No. A Cp 0.84
Stack Thermocouple No. 31 58 A
Filter Holder No. (
Filter Assembly No. £2%
Impinqer Box No. A- /
(
Umbilical/lmpinger Hookup UH-^£3>
Umbilical No. /IJGWH
Meter Box No. Ai 12^
DGM Correction (Y) nfflff
Orifice Meter AH

{'&!& Train B No. M17-B Probe No. B Lenath: 10 ft Nozzle No. M 17- l&Tm Dia. <9-/Y<^ in Pitot Tube No. B Cp 0.84 Stack Thermocouple No. 3158B Filter Holder No. ?- Filter Assembly No. F^ Impinger Box No. B- | Umbilical/lmpinger Hookup UH-^2 — Umbilical No. (J IX?- \ Meter Box No. (Jl\ DGM Correction (Y) (tO(^ Orifice Meter AH@> /'f*^ TT page 1 of. 1 Assumed %CO, /*•? TAJ LfiJ Lcj LoJ LEJ Traverse Point Layout Compass Direction >• North Nozzles are quartz-glass. Time (24 Hr) Pass or Fail Train A Pitot Tube Pressure Measurement System Leak Checks Initial \w> Final tit ttp* Initial Final Initial Final Initial Final Initial Final Train B Pitot Tube Pressure Measurement System Leak Checks Initial lW Final /W $&a Initial Final Initial Final Initial Final Initial Final Train A Sampling System Leak Cnecks Time (24 Hr) Vacuum, in Hg Leak Rate, cfm Initial (W6 iT ,ocfa Final Meter Volume Initial Meter Volume Leak Check Volume Final


-------
   Run No.
   Date
                             Sampling Location  Unit 2A Baahouse Outlet Duct
                             Project No.   104703.1.002.05.01	
                                                                     Operator
                                                              page.
                                                                        of 2_
                                                Sampling Data for Method 17 Train A No.   M17-A
           Sampling
            Time,
   Traverse
    Point
                         Clock
                         Time
                        (24-Hr)
Dry Gas Meter Reading
      (VJ, ft3
                          Initial
                                 Desired
            Actual
Velocity
 Head
 (Ap),
in. H20
 Orifice Pressure
  Differential
     (AH),
    in. H20
Desired  Actual
Stack
Temp.
 It.).
  °F
Dry Gas Meter
 Temperature
                                                                               Inlet
                                                                                          Outlet
              Pump
             Vacuum,
              in. Hg
Silica Gel
Impinger
 Outlet
 Temp.,
   °F
                                                                                     £o_
      Y
                                             &-
                                                                   <2*>
                                                                              S'f
           4J
                        M=_
                                                                                            ^_
                                                                                                   $
                                                                                           3-
                                              o/&
                                                              G--3?
                                                                                         32^.
                &**
                                   0r/(
                                                                                                    4-Z-
                    f*
                                  , 16,
                                                          #3
ML
                                                                      ftoff
                                                                 -Z
                                                                                   &L-
                                                                                            f
                                                                                            •7
                                                                              3"7
                                                                                                 -7
                                                                      &L
                                                Sampling Data for Method 17 Train B No.   M17-B
                              M-
                                                                                                         ^SL
                                                                              22L
                  fft*
                                                                              £3
                                                                                                 -7
                                               0,97
                                                           0,23
                                    a,??
                                                                                     $3
                                    ZZJ'lf
                                                                                          Sf
                                                                       S&3
                                                                                                         •f?
                                               t>#3
                                                                           m-
                                                                      A3
                          •2-Z1,
               i
                                                                                          ££.
                OL
                                                                            t#S
                                                                                     r?
   Remarks and Notes:
   M17DPG2.WPD Septembers. 1999
76
                                             RCA#2 APPENDIX C

-------
                      40 CFR 60, APPENDIX A, METHOD 3B
                       INTEGRATED GAS SAMPLING DATA
Run No..
                  Date
Project No.  104703.1.002.05.01 _
Sample Type (Multi-Point, Single-Point)
Flow Control Device (Valve, Critical Orifice)
Method 5 Meter Box No.
MSB Pump Type  diaohram
MSB Pump No.     A} it
                       Client/Source U.S. EPA / Cogentrix Unit 2A
                       Sampling Location Unit 2A Baghouse Outlet
                       Operator	6
                                       Bag Type  Tedlar
                                       Method 3B Train No. _
                                       MSB Flow Meter Type.
                                       MSB Flow Meter No.
                                            Sample No.
                                           NA	
                                                  NA
                                            rotameter
Desired Sampling Rate	
Leak Check Before Sampling.
Total Sampling Time    "/O
                                  cc/min
Flow Rate, cc/min: Average _
Estimated Total Sample Volume
            3;	  After Sampling
            min  Average Flow Meter Reading
                	 Highest _
                                                             Lowest
                                          liters
  Time
 (24-Hr)
         Flow
         Meter
        Reading
Start
Purge
  Start
Sampling
  Stop
Sampling
Sampling
Remarks and Notes
 Mel
                                                           &
 Hffi
 /tftz
 ffto
        1*
                                                          o
 ftfo
                                                              Mfi- -
M3BSAMP WPD June IS, 1993
                                                                                   77
                            RCA#2 APPENDIX C

-------
  co
s
TJ
o
                                          40 CF/? 60, APPENDIX A, METHOD 3B, GAS ANALYSIS BY ORSAT
                      Run No.
                                  Date
Project No.  104703.1.002.05.01     Sample No. .
Sampling Location   Unit 2A Baghouse Outlet Duct
Analysis Start Time
                                                                      NA
                      Sample Type (Bag, Grab)
                      Analyst   J>
                         Bag
Orsat Leak Check Before Analysis:
Burrete   /Y®     Change in 4 Minutes
Pipettes  x^>	Change in 4 Minutes
Orsat Leak Check After Analysis:
Burrete   >>,/>
3
1 ^>
2 %-T^~
3
Net
Value

/y. '


>5~' <*

3

Actual
Reading
1 /*>.'
2 ;>JJ
3
V^-2.
2 ^2,
3
Net
Value

/#•)


£~'J

Average
Net
Value
(% v/v)

/^>/


<£~J

                                        CO,
                         Acceptance Criteria per Method 3B
                          •   0.3%  v/v     02   >J5%  0.2% v/v
                          ,   0.2%  v/v          <15%  0.3% v/v
               Remarks and Notes:
               M3BANALWPD Septembers, 1999

-------
              40 CFR 60, APPENDIX A, METHOD 17 - PARTICULATE MATTER TRAIN (M17)
                       FIELD LABORATORY TRAIN SET-UP DATA FOR TWO TRAINS

   MRI Project No. 104703.1.002.05.01
     Client/Source: U.S. EPA OAQPS EMAD EMC / Cogentrix Unit 2A
  Source Location: Rocky Mount, North Carolina
Sampling Location: Baghouse (Fabric Filter) Outlet Duct

                                               9	  Impinger Box A No.   <&~'	
                                               £	  Impinger Box B No.    ~~S	
  Run No.  *       Sampling Train A No.
                   Sampling Train B No.
  Set-up person(s):    J.
                                                                               Date:
Transfer to Sampler:
Relinquished By    J
                                     Received By
Date/Time
      TRAIN COMPONENT
                                     REAGENT
 LOADING DATA
                                                                           TRAIN A
                                                                                            TRAIN B
      Sampling Nozzle (Quartz)*

     Filter Assembly and Holder*
                    Filter Type: Whatman QM-A
                Probe  (316 SS)
   Sample Transfer/Vacuum Line
 Male 1st Impinger Inlet Blank-Off
                                                        Nozzle I.D. No.

                                                    Filter Assembly No.

                                                       Filter Holder No-
                                                                             Initial Weights (grams)
         1st Impinger (Mod-GBS) 100-200 mLs ASTM Type I Water
               U-Connector (A)                     ;
            2nd Impinger (GBS) 100-200 mLs ASTM Tyjpe I Water
               U-Connector (B)
         3rd Impinger (Mod-GBS) Empty
               U-Connector (C)
         4th Impinger (Mod-GBS) "200 g indicating silica gel
               U-Connector (D)
         5th Impinger (Mod-GBS) "200 g indicating silica gel
       Impinger Outlet Connector
                                                     Connector I.D. No.
     *  Before and after sampling: Nozzle inlet opening and filter assembly holder outlet opening covered with Teflon® tape, and
        entire filter assembly holder with filter assembly and nozzle wrapped in aluminum foil and placed in Ziploc® bag. 1 st impinger
        inlet sealed with glass blank-off.
Comments:
M17DSUP.WPD May 13, 1999 (rev. M17DSUP3.WPD November 10, 1999]
                                                                                                       79
                                     RCA#2 APPENDIX C

-------
                  40 CFR 60, APPENDIX A, METHOD 17 - PARTICULATE MATTER TRAIN (M17)
                       FIELD LABORATORY SAMPLE RECOVERY DATA FOR TWO TRAINS

       MRI Project No. 104703.1.002.05.01
        Client/Source: U.S. EPA OAQPS EMAD EMC / Cogentrix Unit 2A
      Source Location: Rocky Mount, North Carolina
    Sampling Location: Baghouse (Fabric Filter) Outlet  Duct
     Run No.
Sampling Train A No.
Sampling Train B No..
Transfer for Recovery:
Relinquished By   P, 6fj-f-br>
    Sample recovery person(s):
Weights below are in grams.
	 Received By   J, £
 J. Su.
                                                          Impinger Box A No.   >?">?
                                                          Impinger Box B No.    13-J
                                                               5""j
                                                   Date/Time
                                                                                                 /5VP
                                                                                          Date:
                                             BACK HALF RECOVERIES
                                TRAIN A
Impinger:     1st
Final Wt.
Initial Wt.
 Net Wt.
                           2nd
                3rd
                                                4th & 5th
                                                              1 st
                            6,3     -0,1
    Total Condensate Collected:
    Description and/or color:
                           5/7
                                                  % Blue
                                                                                 TRAIN B
                                        2nd
                                                                                       3rd
                                                                          4th & 5th
                                                                        A 5*    -£>,-2-
                                                                                               30
                                                                                                  *
                                                                            % Blue
                                             FRONT HALF RECOVERIES:
                                TRAIN A
    FILTER ASSEMBLY:
           Sample Number:  -jiS? 102
       PM Description/color:
    TRAIN RINSES:
           Sample Number:
       Components Rinsed*: nozzle, filter holder front
                                                                                TRAIN B
         *  Acetone rinses with brushing 3 times or more until perceivably clean.

    COMMENTS: Acetone rinses are transferred directly to tared Teflon® beaker liners for analysis.
    M17DRCV.WPD May 13, 1999 (rev M17DRCV3.WPD November 10, 19991
80
                                             RCA#2  APPENDIX C

-------
                                 RCA #2 Appendix D
       M17 Field Laboratory Particulate Weight Data
MR]-OPPT\R4703-0:-07 Appendices Covers WPD

-------
                 PARTICULATE MATTER (FRONT-HALF) RINSES ANALYSIS DATA

      MRI Project No.  104703.1.002.05.01
       Client/Source:  U.S. EPA OAQPS EMAD EMC / Cogentrix Unit 2A
     Source Location:  Rocky Mount, North Carolina
   Sampling Location:  Baghouse (Fabric Filter) Outlet Duct

    Sampling Team Leader: Jim Surman                     Analyst:    tJ- •2>Mj	
Beaker Liner Size and Type: 250-mL Teflon®
          Acetone Lot No. BO 363
       Sample Treatment: Acetone samples evaporated at ambient temperature and pressure in an
                         enclosure with HEPA-filtered air; then, desiccated  and weighed to a constant weight.
             Weight Unit: grams
   Run No.   J~-&      Beaker No.     '        Sample No.
         Sample Volume  + Acetone Rinses of Bottle           Beaker Liner + Sample Residue Weiahts
                                                           Gross Wt.         Date          Time
                                              . ^i s\ **J
            Beaker + Liner + Sample + Rinses Wt.
                       Beaker + Liner Tare Wt.
                        Sample  +  Rinses Wt.
            Acetone Wt./0.79 = mLs Acetone:
                     Beaker Liner + Residue Gross Weight used for data entry:
                             Beaker Liner Tare Weight from Tare Weight Data:
                                            Acetone Blank for data entry =  	&	 mg/mL
                                                  Volume for data entry =     ??/.(&	 mLs
   Comments:
C50
Run No. J~&
Sample Volume

Beaker No. £? Samole No.
+ Acetone Rinses of Bottle

3o;»3
Beaker Liner
Gross Wt.

+ Sample Residue Weiahts
Date Time
            Beaker + Liner + Sample + Rinses Wt.
                       Beaker + Liner Tare Wt.
                        Sample  +  Rinses Wt.
            Acetone Wt./0.79 = mLs Acetone:
                     Beaker Liner + Residue Gross Weight used for data entry:
                             Beaker Liner Tare Weight from Tare Weight Data:
                                            Acetone Blank for data entry = 	O_	 mg/mL
                                                  Volume for data entry =    3Sj&      mLs
   Comments:
           3*.
   Run No.   J?-S-)      Beaker No.    3	  Sample No.
         Sample Volume + Acetone Rinses of Bottle            Beaker Liner +  Sample Residue Weiahts
                                                            Gross Wt.         Date           Time
                                               . jf* ** j+             ~
            Beaker + Liner + Sample + Rinses Wt.
                       Beaker + Liner Tare Wt.
                        Sample  +  Rinses Wt.
            Acetone Wt./0.79 = mLs Acetone:
                                            	
                      Beaker Liner + Residue Gross Weight used for data entry:
                             Beaker Liner Tare Weight from Tare Weight Data:
                                             Acetone Blank for data entry  = 	O_	 mg/mL
                                                  Volume for data entry  =    &&&•     mLs
   Comments:
   NOTE: Control iiner and reagent blank weight data and balance check data are documented on other forms.
   M5IPMRIX.WPD June 5, 1998 (rev. M17PMRI3.WPD November 10, 1999)
                                  RCA#2 APPENDIX  D

-------
                  PARTICULATE MATTER (FRONT-HALF) RINSES ANALYSIS DATA

      MRI Project No.  104703.1.002.05.01
        Client/Source:  U.S. EPA OAQPS EMAD EMC / Cogentrix Unit 2A
     Source Location:  Rocky Mount, North Carolina
   Sampling Location:  Baghouse (Fabric Filter) Outlet Duct

    Sampling Team Leader: Jim Surman                     Analyst:     J, £<.4ys9?zir->	
Beaker Liner Size and Type: 250-mL Teflon®
          Acetone Lot No. BO 363
        Sample Treatment: Acetone samples evaporated at ambient temperature and pressure in an
                         enclosure with HEPA-filtered air; then, desiccated and weighed to a constant weight.
             Weight Unit: grams

   Run No.   ff-(3      Beaker No.    ^	  Sample No.
         Sample Volume +  Acetone Rinses of Bottle           Beaker Liner + Sample Residue Weights
                                                ^.        Gross Wt.        Date          Time
           Beaker + Liner + Sample + Rinses Wt.   /ffZ&b        £_.
                      Beaker + Liner Tare Wt.
                       Sample + Rinses Wt.
           Acetone Wt./0.79 = mLs Acetone:
                     Beaker Liner + Residue Gross Weight used for data entry:
                             Beaker Liner Tare Weight from Tare Weight Data:
                                            Acetone Blank for data entry = 	&_	 mg/mL
                                                  Volume for data entry =     ff1^-?     mLs
   Comments:
   Run No.   Zf-Jr      Beaker No.  • =T       Sample No..
         Sample Volume + Acetone Rinses of Bottle           Beaker Liner + Sample Residue Weights
                                                           Gross Wt.        Date          Time
           Beaker + Liner + Sample + Rinses Wt.   S33-7
                      Beaker + Liner Tare Wt.
                       Sample + Rinses Wt.
           Acetone Wt./0.79 = mLs Acetone:
                                           	„__   	
                     Beaker Liner + Residue Gross Weight used for data entry:
                             Beaker Liner Tare Weight from Tare Weight Data:   3*'.
                                            Acetone Blank for data entry = 	&_	 mg/mL
                                                  Volume for data entry =     a&£-7     mLs
   Comments:
   Run No.   C7-.P      Beaker No.     &	  Sample No.
         Sample Volume + Acetone Rinses of Bottle           Beaker Liner + Sample Residue Weights
                                                           Gross Wt.        Date          Time
           Beaker + Liner + Sample + Rinses Wt.
                      Beaker + Liner Tare Wt.
                       Sample + Rinses Wt.
           Acetone Wt./0.79 = mLs Acetone:
                     Beaker Liner + Residue Gross Weight used for data entry:
                             Beaker Liner Tare Weight from Tare Weight Data:
                                            Acetone Blank for data entry =      

S rnLs Comments: NOTE: Control liner and reagent blank weight data and balance check data are documented on other forms. M5IPMRIX.WPD June 5, 1998 (rev M17PMRI3.WPD November 10. 1999) RCA#2 APPENDIX D


-------
                 PARTICULATE MATTER (FRONT-HALF) RINSES ANALYSIS DATA

      MRI Project No.  104703.1.002.05.01
        Client/Source:  U.S. EPA OAQPS EMAD EMC / Cogentrix Unit 2A
     Source Location:  Rocky Mount, North Carolina
   Sampling Location:  Baghouse (Fabric Filter) Outlet Duct

    Sampling Team Leader: Jim Surman                     Analyst:  	tJ
Beaker Liner Size and Type: 250-mL Teflon®
          Acetone Lot No. BO 363
        Sample Treatment: Acetone samples evaporated at ambient temperature and pressure in an
                         enclosure with HEPA-filtered air; then, desiccated and weighed to a constant weight.
             Weight Unit: grams
   Run No.   ^~/9      Beaker No.    "7	  Sample No.,
         Sample Volume  + Acetone Rinses of Bottle           Beaker Liner + Sample Residue Weights
                                                           Gross Wt.        Date          Time
            Beaker + Liner + Sample + Rinses Wt.
                       Beaker + Liner Tare Wt.
                        Sample +  Rinses Wt.
            Acetone Wt./0.79 = mLs Acetone:
                     Beaker Liner + Residue Gross Weight used for data entry:
                             Beaker Liner Tare Weight from Tare Weight Data:
                                            Acetone Blank for data entry =  	£/	 mg/mL
                                                  Volume for data entry =     Z?3,C     mLs
   Comments:
   Run No.   V-/?      Beaker No.     a	  Sample No.
         Sample Volume  + Acetone Rinses of Bottle   ..       Beaker Liner + Sample Residue Weights
                                                           Gross Wt.         Date.          Time
            Beaker + Liner + Sample + Rinses Wt.
                       Beaker + Liner Tare Wt.
                        Sample  +  Rinses Wt.
            Acetone Wt./0.79 = mLs Acetone:
                     Beaker Liner + Residue Gross Weight used for data entry:
                             Beaker Liner Tare Weight from Tare Weight Data:
                                            Acetone Blank for data entry =  	O_	 mg/mL
                                                  Volume for data entry =    ^3,3     mLs
   Comments:
   Run No.   -3~-/-)      Beaker No.	2_	  Sample No.
         Sample Volume + Acetone Rinses of Bottle            Beaker Liner + Sample Residue Weights
                                                            Gross Wt.         Date          Time
            Beaker + Liner + Sample + Rinses Wt.
                       Beaker + Liner Tare Wt.
                        Sample  +  Rinses Wt.
            Acetone Wt./0.79 = mLs Acetone:
                      Beaker Liner + Residue Gross Weight used for data entry:
                             Beaker Liner Tare Weight from Tare Weight Data:
                                            Acetone Blank for data entry = 	Q	  mg/mL
                                                  Volume for data entry =    rV^S1	  mLs
   Comments:
   NOTE: Control liner and reagent blank weight data and balance check data are documented on other forms.
   M5IPMRIX WPD JuneS, 1998 (rev M17PMRI3.WPD November 10, 1999)
                                  RCA#2 APPENDIX D

-------
                  PARTICULATE MATTER (FRONT-HALF) RINSES ANALYSIS DATA

      MRI Project No. 104703.1.002.05.01
        Client/Source: U.S. EPA OAQPS EMAD EMC / Cogentrix Unit 2A
     Source Location: Rocky Mount, North Carolina
   Sampling Location: Baghouse (Fabric Filter) Outlet Duct

    Sampling Team Leader: Jim Surman                     Analyst:    (J, Si4/^j*r**^j*?	
Beaker Liner Size and Type: 250-mL Teflon®
          Acetone Lot No. BO 363
        Sample Treatment: Acetone samples evaporated at ambient temperature and pressure in an
                         enclosure with HEPA-filtered air; then, desiccated and weighed to a constant weight.
             Weight Unit: grams
   Run No.  s5"-5      Beaker No.   SO       Sample No.
         Sample Volume + Acetone Rinses of Bottle            Beaker Liner +  Sample Residue Weights
                                                            Gross Wt,         Date          Time
            Beaker + Liner + Sample + Rinses Wt.
                       Beaker + Liner Tare Wt. .
                        Sample  + Rinses Wt.
            Acetone Wt./0.79 = mLs Acetone:
                                               	
                      Beaker Liner + Residue Gross Weight used for data entry:
                             Beaker Liner Tare Weight from Tare Weight Data:
                                             Acetone Blank for data entry = 	<2	  mg/mL
                                                   Volume for data entry =    3?&,S'      mLs
   Comments:
            3S-                          .   \
   Run No.   ^ "iff      Beaker No.     -^>      Beaker No.    SZi	  Sample No.
          Sample Volume + Acetone Rinses of Bottle           Beaker Liner + Sample Residue Weights
                                                            Gross Wt.         Date          Time
            Beaker + Liner + Sample + Rinses Wt.   sS'J.^       ^3 .
                       Beaker + Liner Tare Wt. _
                        Sample + Rinses Wt. _
            Acetone Wt./0.79 = mLs Acetone: _
                      Beaker Liner + Residue Gross Weight used for data entry:
                              Beaker Liner Tare Weight from Tare Weight Data:
                                             Acetone Blank for data entry =       0	 mg/mL
                                                   Volume for data entry =    S'J-'J      mLs
   Comments:
    NOTE: Control liner and reagent blank weight data and balance check data are documented on other forms.
   M5IPMRIX.WPD June 5. 1998 (rev. M17PMRI3.WPD November 10, 19991
                                        RCA#2 APPENDIX D

-------
                 PARTICULATE MATTER (FRONT-HALF) RINSES ANALYSIS DATA

      MRI Project No.  104703.1.002.05.01
       Client/Source:  U.S. EPA OAQPS EMAD EMC / Cogentrix Unit 2A
     Source Location:  Rocky Mount, North Carolina
   Sampling Location:  Baghouse (Fabric Filter) Outlet Duct

    Sampling Team Leader: Jim Surman                     Analyst:     J, Su^m^t?	
Beaker Liner Size and Type: 250-mL Teflon®
          Acetone Lot No. BO 363
       Sample Treatment: Acetone samples evaporated at ambient temperature and pressure in an
                         enclosure with HEPA-filtered air; then, desiccated and weighed to a constant weight.
             Weight Unit: grams
   Run No.    "7-s?      Beaker No.    S3       Sample No.
         Sample Volume  + Acetone Rinses of Bottle           Beaker Liner + Sample Residue Weiahts
                                                           Gross Wt.        Date          Time
            Beaker + Liner + Sample + Rinses Wt.
                       Beaker + Liner Tare Wt.
                        Sample + Rinses Wt.
            Acetone Wt./0.79 = mLs Acetone:
                     Beaker Liner + Residue Gross Weight used for data entry:
                             Beaker Liner Tare Weight from Tare Weight Data:
                                            Acetone Blank for data entry =  	&.	 mg/mL
                                                  Volume for data entry =    c?!/-^	 mLs
   Comments:                                 •                  :
            -56,
   Run No.     *? -3     Beaker No.    ^V       Sample No..
         Sample Volume  + Acetone Rinses of Bottle    .     -   Beaker Liner + Sample Residue Weiahts
                                              .   . :. _      Gross Wt.        Date          Time
            Beaker + Liner + Sample + Rinses Wt. ,
                       Beaker + Liner Tare Wt. .
                        Sample  +  Rinses Wt. .
            Acetone Wt./0.79 = mLs Acetone:
                     Beaker Liner + Residue Gross Weight used for data entry:
                             Beaker Liner Tare Weight from Tare Weight Data:
                                            Acetone Blank for data entry =  	£_	 mg/mL
                                                  Volume for data entry =    ff&~.*J      mLs
   Comments:
   Run No.   $-J9      Beaker No.     /£>"     Sample No.   3
         Sample Volume  + Acetone Rinses of Bottle            Beaker Liner + Sample Residue Weiahts
                                                 ^ ^      Gross Wt.         Date           Time
            Beaker + Liner + Sample + Rinses Wt.
                       Beaker + Liner Tare Wt.   /f>^>"3>      3
                        Sample +  Rinses Wt. _
            Acetone Wt./0.79 = mLs Acetone:
                     Beaker Liner + Residue Gross Weight used for data entry:
                             Beaker Liner Tare Weight from Tare Weight Data:
                                            Acetone Blank for data entry =  	£/_	 mg/mL
                                                  Volume for data entry =     3&s'?     mLs
   Comments:
   NOTE: Control liner and reagent blank weight data and balance check data are documented on other forms.
   M5IPMRIX.WPD June 5, 1998 (rev M17PMRI3.WPD November 10, 1999)
                                  RCA#2 APPENDIX D

-------
                  PARTICULATE MATTER (FRONT-HALF) RINSES ANALYSIS DATA

      MRI Project No. 104703.1.002.05.01
        Client/Source: U.S. EPA OAQPS EMAD EMC / Cogentrix Unit 2A
     Source Location: Rocky Mount, North Carolina
   Sampling Location: Baghouse (Fabric Filter) Outlet Duct

    Sampling Team Leader: Jim Surman                     Analyst:     tJ* £+-*r's-r*£>sf	
Beaker Liner Size and Type: 250-mL Teflon®
          Acetone Lot No. BO 363
        Sample Treatment: Acetone samples evaporated at ambient temperature and pressure in an
                         enclosure with HEPA-filtered air; then, desiccated and weighed to a constant weight.
             Weight Unit: grams
           3?
   Run No.    8~£      Beaker No.    S6>	  Sample No.  3?S03
         Sample Volume  + Acetone Rinses of Bottle            Beaker Liner + Sample Residue Weiahts
                                                            Gross Wt.         Date           Time
           Beaker + Liner + Sample + Rinses Wt.
                       Beaker + Liner Tare Wt.
                        Sample  +  Rinses Wt.
            Acetone Wt./0.79 = mLs Acetone:
                     Beaker Liner + Residue Gross Weight used for data entry:
                             Beaker Liner Tare Weight from Tare Weight Data:
                                            Acetone Blank for data entry =       0	 mg/mL
                                            \      Volume for data entry =    £*9.7	 mLs
   Comments:                                                 i
   Run No.   *?-&      Beaker No.    s/    :-   Sample No.
         Sample Volume  + Acetone Rinses of Bottle           Beaker Liner + Sample Residue Weiahts
                                               	       Gross Wt.         Date          Time
            Beaker + Liner + Sample + Rinses Wt.
                       Beaker + Liner Tare Wt.
                        Sample +  Rinses Wt.
            Acetone Wt./0.79 = mLs Acetone:
                     Beaker Liner + Residue Gross Weight used for data entry:
                             Beaker Liner Tare Weight from Tare Weight Data:
                                            Acetone Blank for data entry =  	^	 mg/mL
                                                  Volume for data entry =    jZ>£jZ2.    mLs
   Comments:
   Run No.    7 -&      Beaker No.     '&       Sample No.
         Sample Volume  + Acetone Rinses of Bottle           Beaker Liner + Sample Residue Weiahts
                                               .,.»,-,.~       Gross Wt.         Date           Time
            Beaker + Liner + Sample + Rinses Wt.
                      Beaker + Liner Tare Wt.
                        Sample +  Rinses Wt.
            Acetone Wt./0.79 = mLs Acetone:
                                             	
                     Beaker Liner + Residue Gross Weight used for data entry:
                             Beaker Liner Tare Weight from Tare  Weight Data:
                                            Acetone Blank for data entry =  	&_	 mg/mL
                                                  Volume for data entry =     £?'2'7     mLs
   Comments:
   NOTE: Control liner and reagent blank weight data and balance check data are documented on other forms.
                                                                                          I"
   M5IPMRIX.WPD June 5. 1998 (rev. M17PMRI3.WPD November 10. 1999)
                                       RCA#2  APPENDIX D

-------
                 PARTICULATE MATTER (FRONT-HALF) RINSES ANALYSIS DATA

      MRI Project No.  104703.1.002.05.01
        Client/Source:  U.S. EPA OAQPS EMAD EMC / Cogentrix Unit 2A
     Source Location:  Rocky Mount, North Carolina
   Sampling Location:  Baghouse (Fabric Filter) Outlet Duct

    Sampling Team Leader: Jim Surman                     Analyst:  	JJ.
Beaker Liner Size and Type: 250-mL Teflon®
          Acetone Lot No. BO 363
        Sample Treatment: Acetone samples evaporated at ambient temperature and pressure  in an
                         enclosure with HEPA-filtered air; then, desiccated and weighed to a constant weight.
             Weight Unit: grams
   Run No.   S&-/2     Beaker No.   S9        Sample No.
         Sample Volume  + Acetone Rinses of Bottle           Beaker Liner + Sample Residue Weights
                                                           Gross Wt.        Date          Time
                                              . j».t r\
            Beaker + Liner + Sample + Rinses Wt.
                      Beaker + Liner Tare Wt.
                        Sample +  Rinses Wt.
            Acetone Wt./0.79 = mLs Acetone:
                     Beaker Liner + Residue Gross Weight used for data entry:  ^
                             Beaker Liner Tare Weight from Tare Weight Data:  3. z5~S
                                            Acetone Blank for data entry = 	^	 mg/mL
                                              =     Volume for data entry =    &J.£	 mLs
   Comments:
   Run No.  S&-&      Beaker No.   *(&      ; Sample No.
         Sample Volume  + Acetone Rinses of Bottle           Beaker Liner + Sample Residue Weights
                                                           Gross Wt.         Date          Time
            Beaker + Liner + Sample + Rinses Wt.
                       Beaker + Liner Tare Wt.   4O.f
                        Sample +  Rinses Wt.
            Acetone Wt./0.79 = mLs Acetone:
                      Beaker Liner + Residue Gross Weight used for data entry:  3>
                             Beaker Liner Tare Weight from Tare Weight Data:
                                            Acetone Blank for data entry =   *s  O	 mg/mL
                                                  Volume for data entry = /l>iiP^£*&.•¥ mLs
   Comments:                                                            /
   Run No.   / )~ri      Beaker No.    a*/	  Sample No.
         Sample Volume + Acetone Rinses of Bottle            Beaker Liner + Sample Residue Weights
                                                            Gross Wt.         Date           Time
            Beaker + Liner + Sample + Rinses Wt.   SSZi.'r      3i S3 SSL
                       Beaker + Liner Tare Wt.
                        Sample  +  Rinses Wt.
            Acetone Wt./0.79 = mLs Acetone: .
                      Beaker Liner +  Residue Gross Weight used for data entry:
                             Beaker Liner Tare Weight from Tare Weight Data:
                                             Acetone Blank for data entry  = 	O_	 mg/mL
                                                   Volume for data entry  =     ^^_S     mLs
   Comments:
   NOTE: Control liner and reagent blank weight data and balance check data are documented on other forms.
   M5IPMRIX.WPD June 5, 1998 (rev. M17PMRI3.WPD November 10, 19991
                                  RCA#2 APPENDIX D

-------
                  PARTICULATE MATTER (FRONT-HALF) RINSES ANALYSIS DATA

      MRI Project No. 104703.1.002.05.01
        Client/Source: U.S. EPA OAQPS EMAD EMC / Cogentrix Unit 2A
     Source Location: Rocky Mount, North Carolina
   Sampling Location: Baghouse (Fabric Filter) Outlet Duct

    Sampling Team Leader: Jim Surman                     Analyst:     -7	
Beaker Liner Size and  Type: 250-mL Teflon®
          Acetone Lot No. BO 363
        Sample Treatment: Acetone samples evaporated at ambient temperature and pressure in an
                         enclosure with HEPA-filtered air; then, desiccated and weighed to a constant weight.
             Weight Unit: grams
   Run No.   SJ-&      Beaker No.   ZZ-       Sample No.
         Sample Volume + Acetone Rinses of Bottle           Beaker Liner + Sample Residue Weights
                                                           Gross Wt.         Date          Time
            Beaker + Liner + Sample + Rinses Wt.
                       Beaker + Liner Tare Wt.
                        Sample +  Rinses Wt.
            Acetone Wt./0. 79 = mLs Acetone:     3?,2-
                     Beaker Liner + Residue Gross Weight used for data entry:
                             Beaker Liner Tare Weight from Tare Weight Data:  3;
                                            Acetone Blank for data entry =  	£?	 mg/mL
                                                  Volume for data entry =      33-Z—   mLs
   Comments:
   Run No.   /&-J9     Beaker No.   xvJ?       Sample No.
         Sample Volume + Acetone Rinses of Bottle            Beaker Liner + Sample Residue Weights
                                                            Gross Wt.         Date          Time
                                                _ —«  t
            Beaker + Liner + Sample + Rinses Wt.
                       Beaker + Liner Tare Wt.
                        Sample  +  Rinses Wt.
            Acetone Wt./0.79 = mLs Acetone:
                      Beaker Liner + Residue Gross Weight used for data entry:
                             Beaker Liner Tare Weight from Tare Weight Data:
                                            Acetone Blank for data entry =      O	 mg/mL
                                                  Volume for data entry =    £*).*?     mLs
   Comments:
   Run No.  /&-&     Beaker No.    &*+•       Sample No.
         Sample Volume + Acetone Rinses of Bottle            Beaker Liner +  Sample Residue Weights
                                                            Gross Wt.         Date          Time
                                               . . _ ^*
            Beaker + Liner + Sample + Rinses Wt.
                       Beaker + Liner Tare Wt.   /
-------
                  PARTICULATE MATTER (FRONT-HALF) RINSES ANALYSIS DATA

      MRI Project No. 104703.1.002.05.01
        Client/Source: U.S. EPA OAQPS EMAD EMC / Cogentrix Unit 2A
     Source Location: Rocky Mount, North Carolina
   Sampling Location: Baghouse (Fabric Filter) Outlet Duct

    Sampling Team Leader: Jim Surman                     Analyst:
Beaker Liner Size and Type: 250-mL Teflon®
          Acetone Lot No. BO 363
        Sample Treatment: Acetone samples evaporated at ambient temperature and pressure in an
                         enclosure with HEPA-filtered air; then, desiccated and weighed to a constant weight.
             Weight Unit: grams
   Run No.   S3~J?     Beaker No.              Sample No.
         Sample Volume +  Acetone Rinses of Bottle           Beaker Liner + Sample Residue Weights
                                                    ^,     Gross Wt.         Date          Time
            Beaker + Liner + Sample + Rinses Wt.   /%%v^>
                      Beaker + Liner Tare Wt.
                       Sample + Rinses Wt.
            Acetone Wt./0.79 = mLs Acetone:
                     Beaker Liner + Residue Gross Weight used for data entry:
                             Beaker Liner Tare Weight from Tare Weight Data:
                                            Acetone Blank for data entry = 	«2	  mg/mL
                                                  Volume for data entry =     &&.)      mLs
   Comments:                         .
   Run No.   S&-&      Beaker No.  Z?£c	  Sample No.
         Sample Volume + Acetone Rinses of Bottle           Beaker Liner + Sample Residue Weights
                                                           Gross Wt.         D.ate          Time
           Beaker + Liner + Sample + Rinses Wt.   /&&-8
                      Beaker + Liner Tare Wt.   /d^S?
                       Sample + Rinses Wt.
            Acetone Wt./0.79 = mLs Acetone:
                     Beaker Liner + Residue Gross Weight used for data entry:
                             Beaker Liner Tare Weight from Tare Weight Data:
                                            Acetone Blank for data entry =      O	  mg/mL
                                                  Volume for data entry =    jj2£7«»*      mLs
   Comments:
   Run No.	  Beaker No.	  Sample No.
         Sample Volume + Acetone Rinses of Bottle           Beaker Liner  + Sample Residue Weights
                                                           Gross Wt.         Date          Time
           Beaker + Liner + Sample + Rinses Wt. 	    	   	    	
                      Beaker + Liner Tare Wt. 	    	   	    	
                       Sample + Rinses Wt. 	    	   	    	
           Acetone Wt./0.79 = mLs Acetone: 	    	   	    	
                     Beaker Liner + Residue Gross Weight used for data entry:
                             Beaker Liner Tare Weight from Tare Weight Data:
                                            Acetone Blank for data entry = 	  mg/mL
                                                  Volume for data entry = 	  mLs
  Comments:
  NOTE: Control liner and reagent blank weight data and balance check data are documented on other forms.
  MSIPMRIX.WPD June 5. 1998 (rev M17PMHI3.WPD November 10. 19991
                                 RCA#2 APPENDIX D

-------
                 PARTICULATE MATTER IN FILTER ASSEMBLY ANALYSIS DATA

     MRI Project No. 104703.1.002.05.01
       Client/Source: U.S. EPA OAQPS EMAD EMC / Cogentrix Unit 2A
    Source Location: Rocky Mount, North Carolina
   Sampling Location: Baghouse (Fabric Filter) Outlet Duct

   Sampling Team Leader: Jim Surman                    Analyst:   c/
      Filter Size and Type: 47mm diameter, Whatman QM-A quartz glass fiber filter
            Filter Lot No. 25460
   Assembly Components: filter, aluminum foil gasket, and 316 stainless steel filter support
Filter Assembly Treatment: HydL at lUb "L fui 3-l-njulST desiccate and weigh to a constant weight.
            Weight Unit: grams                1&
  Run No.  /-v#      Assembly No.    / _  Sample No.
              Gross Wt.        Date          Time        Comments:
                 Assembly Gross Weight used for data entry:  *-*••
               Assembly Tare Weight from Tare Weight Data:  J
  Run No.  A-*? _ Assembly No.    ^ _  Sample No.
              Gross Wt.        Date        ...Time :. .      Comments:
              3,
                 Assembly Gross Weight used for data entry:
               Assembly Tare Weight from Tare Weight Data:   3. "<3&S
  Run No.  #-<&        Assembly No.    -3 _  Sample No.
              Gross Wt.        Date          Time        Comments:
              3.
                 Assembly Gross Weight used for data entry:
               Assembly Tare Weight from Tare Weight Data:
  NOTE: Control and blank assembly weight data and balance check data are documented on other forms.
  M5IPMFIX.WPD JuneS. 1998 (rev M17PMFI3.WPD November 10. 1999}
                                       RCA#2 APPENDIX D

-------
                 PARTICULATE MATTER IN FILTER ASSEMBLY ANALYSIS DATA

     MRI Project No.  104703.1.002.05.01
       Client/Source:  U.S. EPA OAQPS EMAD EMC / Cogentrix Unit 2A
    Source Location:  Rocky Mount, North Carolina
   Sampling Location:  Baghouse (Fabric Filter) Outlet Duct

   Sampling Team Leader: Jim Surman                   Analyst:            Sample No.
              Gross Wt.        Date          Time        Comments:
                 Assembly Gross Weight used for data entry:
               Assembly Tare Weight from Tare Weight Data:
  NOTE: Control and blank assembly weight data and balance check data are documented on other forms.
  M6IPMFIX.WPD June 5. 1998 Irev. M17PMFI3.WPD November 10. 1999)
                                                                                                  11
                                RCA#2 APPENDIX D

-------
                          PARTICULATE MATTER IN FILTER ASSEMBLY ANALYSIS DATA

              MRI Project No.  104703.1.002.05.01
                Client/Source:  U.S. EPA OAQPS EMAD EMC / Cogentrix Unit 2A
             Source Location:  Rocky Mount, North Carolina
           Sampling Location:  Baghouse (Fabric Filter) Outlet Duct

           Sampling Team Leader:  Jim Surman                   Analyst:   o/,
              Filter Size and Type:  47mm diameter, Whatman QM-A quartz glass fiber filter
                     Filter Lot No.  25460
           Assembly Components:  filter, aluminum foil gasket, and 316 stainless steel filter support
         Filter Assembly Treatment:  I lent at 105-^C for 3 hows, desiccate and weigh to a constant weight.
                     Weight Unit:  grams                $& i\ljt>)W
           Run No.    V-i/9      Assembly No.     "7        Sample No.
                       Gross Wt.         Date          Time        Comments:
                          Assembly Gross Weight used for data entry:
                       Assembly Tare Weight from Tare Weight Data:
                  33                              •
           Run No.  4-8       Assembly No.    S _ '  Sample No.
                       Gross Wt.        Date   .       Time   :     Comments:
                          Assembly Gross Weight used for data entry:
                       Assembly Tare Weight from Tare Weight Data:
           Run No.   &-S9      Assembly No.     9 _  Sample No.
                       Gross Wt.        Date          Time        Comments:
                       3,3**)
                          Assembly Gross Weight used for data entry:
                       Assembly Tare Weight from Tare Weight Data:
           NOTE: Control and blank assembly weight data and balance check data are documented on other forms.
          M5IPMFIX.WPD June 5, 1998 (rev. M17PMFI3.WPD November 10. 19991
12
                                              RCA#2 APPENDIX D

-------
                 PARTICULATE MATTER IN FILTER ASSEMBLY ANALYSIS DATA

     MRI Project No. 104703.1.002.05.01
       Client/Source: U.S. EPA OAQPS EMAD EMC / Cogentrix Unit 2A
    Source Location: Rocky Mount, North Carolina
   Sampling Location: Baghouse (Fabric Filter) Outlet Duct

   Sampling Team Leader: Jim Surman                   Analyst:   *J. <
     Filter Size and Type: 47mm diameter, Whatman QM-A quartz glass fiber filter
            Filter Lot No. 25460
   Assembly Components: filter, aluminum foil gasket, and 316 stainless steel filter support
Filter Assembly Treatment: +reaTdl lOb "LI lul 'J hwuts, desiccate and weigh to a constant weight.
            Weight Unit: grams                 f-3 :
  Run No.    3-J5      Assembly No.    /& _  Sample No.
              Gross Wt.         Date          Time        Comments:
                 Assembly Gross Weight used for. data entry:
               Assembly Tare Weight from Tare Weight Data:
                                         .  .  . = •  :
  Run No.   ^V?      Assembly No.     M        Sample No,
              Gross Wt.        Date          Time        Comments:
                 Assembly Gross Weight used for data entry:
               Assembly Tare Weight from Tare Weight Data:
  Run No.   &> ~&       Assembly No.    S^Z       Sample No.
              Gross Wt.        Date          Time        Comments:
                 Assembly Gross Weight used for data entry:   *=*"
               Assembly Tare Weight from Tare Weight Data:
  NOTE: Control and blank assembly weight data and balance check data are documented on other forms.
                                                                                 u
  M5IPMFIX.WPD June 5, 1998 (rev M17PMF13.WPD November 10, 1999)
                                                                                                   13
                                 RCA#2 APPENDIX D

-------
                          PARTICULATE MATTER IN FILTER ASSEMBLY ANALYSIS DATA

              MRI Project No. 104703.1.002.05.01
                Client/Source: U.S. EPA OAQPS EMAD EMC / Cogentrix Unit 2A
             Source Location: Rocky Mount, North Carolina
           Sampling Location: Baghouse (Fabric Filter) Outlet Duct

           Sampling Team Leader: Jim Surman                    Analyst:     t-A
              Filter Size and Type: 47mm diameter, Whatman QM-A quartz glass fiber filter
                     Filter Lot No. 25460
           Assembly Components: filter, aluminum foil gasket, and 316 stainless steel filter support
         Filter Assembly Treatment: ^Heat at 105 "C toi 3 IH-HUS, desiccate and weigh to a constant weight.
                     Weight Unit: grams                  »|3oM
           Run No.   7-S3      Assembly No.    X^       Sample No.
                       Gross Wt.         Date          Time       Comments:
                          Assembly Gross Weight used for data entry:  3.
                        Assembly Tare Weight from Tare Weight Data:  •
           Run No.    7-8     Assembly No.   /^        Sample No.
                       Gross Wt.         Date        . Time ......   Comments:

                                     S'J/ffo
                          Assembly Gross Weight used for data entry:
                        Assembly Tare Weight from Tare Weight Data:  3* "3 7&O
           Run No.     0-S)     Assembly No.    S^S*      Sample No.
                       Gross Wt.         Date         Time        Comments:
                          Assembly Gross Weight used for data entry:   J,-
                        Assembly Tare Weight from Tare Weight Data:  3.
           NOTE: Control and blank assembly weight data and balance check data are documented on other forms.
           MSIPMFIX.WPD June 5, 1998 (rev M17PMFI3.WPD November 10, 19991
14
                                               RCA#2 APPENDIX D

-------
                 PART1CULATE MATTER IN FILTER ASSEMBLY ANALYSIS DATA

      MRI Project No. 104703.1.002.05.01
       Client/Source: U.S. EPA OAQPS EMAD EMC / Cogentrix Unit 2A
     Source Location: Rocky Mount, North Carolina
   Sampling Location: Baghouse (Fabric Filter) Outlet Duct

   Sampling Team Leader: Jim Surman                    Analyst:    <)•
      Filter Size and Type: 47mm diameter, Whatman QM-A quartz glass fiber filter
            Filter Lot No. 25460
   Assembly Components: filter, aluminum foil gasket, and 316 stainless steel filter support
Filter Assembly Treatment: rHear at I Ob U(J TGI 3 liuw*, desiccate and weigh to a constant weight.
            Weight Unit: grams                i \bo~IW
           37
  Run No.   %-&       Assembly No.    SCe _  Sample No.
              Gross Wt.        Date          Time        Comments:
              3..
                 Assembly Gross Weight used for data entry:   •& '2*2 "3 S
               Assembly Tare Weight from Tare Weight Data:   3.-  '
           __

  Run No.   9-/?      Assembly No.   /7        Sample No.
              Gross Wt.         Date          Time        Comments:
                 Assembly Gross Weight used for data entry:
               Assembly Tare Weight from Tare Weight Data:
  Run No.   9-J&      Assembly No.    /
-------
                          PARTICULATE MATTER IN FILTER ASSEMBLY ANALYSIS DATA
              MRI Project No.  104703.1.002.05.01
                Client/Source:  U.S. EPA OAQPS EMAD EMC / Cogentrix Unit 2A
             Source Location:  Rocky Mount, North Carolina
           Sampling Location:  Baghouse (Fabric Filter)  Outlet Duct

           Sampling Team Leader: Jim Surman                   Analyst:   cA
              Filter Size and Type:  47mm diameter, Whatman QM-A quartz glass fiber filter
                    Filter Lot No.  25460
           Assembly Components:  filter, aluminum foil gasket,  and 316 stainless steel filter support
         Filter Assembly Treatment:  Hoot at 1-90 "C fill  3 hoUr> desiccate and weigh to a constant weight.
                    Weight Unit:  grams               ^
           Run No.   /J-^9      Assembly No.     S9       Sample No.
                       Gross Wt.         Date          Time        Comments:

                  -^/i 3
                          Assembly Gross Weight used for data entry:   &••
                       Assembly Tare Weight from Tare Weight Data:
           Run No.    /'
-------
                 PARTICULATE MATTER IN  FILTER ASSEMBLY ANALYSIS DATA

     MRI Project No. 104703.1.002.05.01
       Client/Source: U.S. EPA OAQPS EMAD EMC / Cogentrix Unit 2A
    Source Location: Rocky Mount, North Carolina
   Sampling Location: Baghouse (Fabric Filter) Outlet Duct

   Sampling Team Leader: Jim Surman                   Analyst:     
-------
                          PARTICULATE MATTER IN  FILTER ASSEMBLY ANALYSIS DATA

              MRI Project No.  104703.1.002.05.01
                Client/Source:  U.S. EPA OAQPS EMAD EMC / Cogentrix Unit 2A
             Source Location:  Rocky Mount, North Carolina
           Sampling Location:  Baghouse (Fabric Filter) Outlet  Duct

           Sampling Team Leader: Jim Surman                   Analyst:    *J->
              Filter Size and Type:  47mm diameter, Whatman QM-A quartz glass fiber filter
                     Filter Lot No.  25460
           Assembly Components:  filter, aluminum foil gasket, and 316 stainless steel filter support
         Filter Assembly Treatment:  neat ai 'liffi PC fui 3imycs. desiccate and weigh to a constant weight.
                     Weight Unit:  grams                 ^nb'ty*
           Run No.  S3~,&      Assembly No.   tf^       Sample No.
                       Gross Wt.         Date          Time        Comments:
                          Assembly Gross Weight used for data entry:
                       Assembly Tare Weight from Tare Weight Data:
           Run No.   /^-
-------
                           PARTICULATE MATTER CONTROLS ANALYSIS  DATA

   MRI Project No.  104703.1.002.05.01
     Client/Source:  U.S. EPA OAQPS EMAD EMC / Cogentrix Unit 2A
  Source Location:  Rocky Mount, North Carolina
Sampling Location:  Baghouse (Fabric Filter) Outlet Duct

 Sampling Team Leader: Jim Surman                             Analyst:    *J'
               Balance: AND ER-120A, MRI #12007
           Weight Unit: grams

Control Filter Assembly Weights & Balance Checks:
Assembly No.   33                   NIST Weight:       Assembly No.   ****                   NIST Weight:
Original Tare Wt.:  ..?- '3 3¥(t>              1 gram         Original Tare Wt.:  •?-> '38^'?              1 gram

 Current Wt.       Date        Time    Balance Reading     Current Wt.       Date       Time    Balance Reading

 3,3335~    /JJJ9J&?     0330   	,
 3' 331k     //Jfft>}99   S60?      J.t>t?£>£>
Comments:
Control Beaker Liner Weights & Balance Checks:
Beaker No.   33                       NIST Weight:       Beaker No.   ->y                       NIST Weight:
Original Tare Wt.:  3^ •J^&b               1 gram        Original Tare Wt.:  &-• ~?&S'?              1 gram

 Current Wt.       Date        Time     Balance Reading     Current Wt.       Date        Time     Balance Reading

  3,-
 3
                             3230
  A-'MS?     /'/MJW
Comments:
Controls are filter assemblies and beaker liners selected from the original prepared lots that are used for sampling and analysis. They
are processed along with the assemblies and liners containing samples during analysis, i.e., they are.heated, desiccated, and weighed
along with the assemblies and liners containing samples.  The results are not used for correcting analytical data, but are useful in
monitoring changes between original tare weights and weights obtained during analysis of samples. Significant changes could
indicate problems in maintaining relatively constant environmental conditions in the laboratory, processing procedures not replicating
those used when tare weights were obtained, instrumentation calibration drift, and desiccant deterioration.

Each time filter assemblies  or beaker liners are weighed, the balance is checked for accuracy by weighing NIST certified weights
approximating the weights of the assemblies or liners.


M5IPMCOX.WPD June 5. 1998 (rev. M17PMC03.WPO November 10. 19991                                            ]]!''''



                                                                                                            19
                                      RCA#2 APPENDIX D

-------
                             PARTICULATE MATTER REAGENT BLANK ANALYSIS DATA
               MRI Project No.  104703.1.002.05.01
                Client/Source:  U.S. EPA OAQPS EMAD EMC / Cogentrix Unit 2A
              Source Location:  Rocky Mount, North Carolina
            Sampling Location:  Baghouse (Fabric Filter) Outlet Duct
                                                     Analyst:    cA
            Sampling Team Leader: Jim Surman
        Beaker Liner Size and Type: 250-mL Teflon®
                  Acetone Lot No. BO 363
                Sample Treatment: Acetone samples evaporated at ambient temperature and pressure in an
                                 enclosure with HEPA-filtered air; then, desiccated and weighed to a  constant weight.
               Filter Size and Type: 47mm diameter, Whatman QM-A quartz glass fiber filter
                     Filter Lot No. 25460
            Assembly Components: filter, aluminum foil gasket, 316 stainless steel filter support
         Filter Assembly Treatment: •l.leamJ Jl  10G °C for 3 hours,  desiccated and weighed to a constant weight.
          Weight Unit: grams

Acetone Blank Determination: For Run No.(s)
                                                     Beaker No.
           A.
                    Acetone Reagent Blank Sample Volume
      Beaker + Liner + Acetone Sample Wt.
                   Beaker + Liner Tare Wt.
                     Acetone Sample Wt.
         Acetone Wt./0.79 = mLs Acetone:
                                                                                      Sample No.
                                                        Beaker Liner
                                                         Gross Wt.
                                                                               + Sample Residue Weights
                                                                                      Date           Time
                                           SC&.J
                                            87,3
                                                                    3 *
           B.
           Comments:
           Beaker Liner +  Residue Gross Weight used for blank determination:
                          Beaker Liner Tare Weight from Tare Weight Data:
                                     Net Weight of Residue in beaker liner:
                                Acetone Blank (B x 1000/A) for.data entry:
                                                                                       O
                                                                                                mg/mL
Filter Assembly Blank Determination: For Run No.(s)

   Gross Wt.        Date          Time        Comments:
                                                       Assembly No.
A.
B.
                                  Assembly Gross Weight used for blank determination:
                                        Assembly Tare Weight from Tare Weight Data:
                                 Net Assembly Weight Difference (A - B) for data entry:
                                                [retain minus sign if value is negative]
                                                                                        Sample No.
           NOTE:  Control liner and filter assembly weights and balance check data are documented on another form.
                                                                                          II
           M5IPMBLX.WPD June 5, 1998 (rev. Ml 7PMBL3.WPD November 10, 19991
20
                                                RCA#2 APPENDIX D

-------
             40 CFR 60, APPENDIX A, METHOD 17 -  PARTICULATE MATTER TRAIN (M17)
                              FIELD REAGENT BLANK  PREPARATION DATA

       MRI Project No.  104703.1.002.05.01
        Client/Source:  U.S. EPA OAQPS EMAD EMC / Cogentrix Unit 2A
      Source Location:  Rocky Mount, North Carolina
    Sampling Location:  Baghouse (Fabric Filter) Outlet Duct

  Blank(s)  Prepared By:       J. ^Uj'jivSirr	  Date:  /S/J6/99	

Weights below are in grams.
                                               Sample         Bottle Tare       Bottle Gross      Net Sample
	Reagent Blank Description	        Number           Weiaht          Weiaht          Weiaht

Acetone for particulate matter
         Volume needed: 100 mLs
            Lot Number: BO 363

Filter Assembly for particulate matter                ;           J'srts' -fas' &»
                  Type: Whatman QM-A          .'-,'
  Filter Assembly Number:    
-------
                                       BEAKER LINER TARE WEIGHT DATA
                MRI Project No.  104703.1.002.05.01
         Sampling Team Leader:  Jim Surman                        Analyst:  	•
     Beaker Liner Size and Type:  250-mL Teflon®
         Beaker Liner Treatment:  Wash to clean, rinse with Dl water, dry at 105 "C,  insert into glass beakers previously
                               cleaned in the same manner, desiccate for 24 hours, and weigh to a constant.
                   Weight Unit:  grams
                Date:
         Time Started:
      Balance Check before beaker liners are weighed:
        Balance Used:
        Weight Value:        /^	         Sty	   	
       Balance Reads:      />&&*&	       AM0&	   	
                                                                                            Average Weight
      Beaker Liner in                                                                          or Weight to be
      Beaker I.D. No.      First Weighing         Second Weighing         Third Weighing        Used as the Tare
                         3,6,93 •/
                        3, S3 ??	     3,833$          	     3,33X3
                                               3.3118
      Balance Check after beaker liners are weighed:
       Balance Reads:
      COMMENTS:
                                                                                            3,3937
      M5IBEAKX.WPD June 4, 1998 Irev M17BEAK3.WPD November 10, 19991
22                                             RCA#2 APPENDIX  D

-------
                                  BEAKER LINER TARE WEIGHT DATA
          MRI Project No.  104703.1.002.05.01
    Sampling Team Leader:  Jim Surman                        Analyst:  	
Beaker Liner  Size and Type:  250-mL Teflon®
   Beaker Liner Treatment:  Wash to clean, rinse with Dl water, dry at 105 °C, insert into glass beakers previously
                          cleaned in the same manner, desiccate for 24 hours, and weigh to a constant.
             Weight Unit:  grams
          Date:  _
   Time Started:
Balance Check before beaker liners are weighed:
   Balance Used:  /9XP  ££-
   Weight Value:  	/fV"
  Balance Reads:       ••
                                                                                         Average Weight
Beaker Liner in                                                                            or Weight to be
Beaker I.D. No.       First Weighing          Second Weighing         Third Weighing         Used as the Tare
     23
                   3. '
                   3 ,<*
                   3,
    33
Balance Check after beaker liners are weighed:
 Balance Reads:      /.£>&
-------
                                     FILTER ASSEMBLY TARE WEIGHT DATA
                MRI Project No.  104703.1.002.05.01
         Sampling Team Leader:  Jim Surman
                                                         Analyst:
            Filter Size and Type:  47mm diameter, Whatman QM-A quartz glass fiber filter
                  Filter Lot No.  25460
         Assembly Components:  filter, aluminum foil gasket, and 316 stainless steel filter support
      Filter Assembly Treatment:  Heat at 105 °C for 3 hours, desiccate, and weigh to a constant weight.
                  Weight Unit:  grams
                Date:      ''  ''  	              '	   	
        Time Started:  	
      Assemblv No.
           1
JL
          it
          it
          I*
          0
      Balance Check before filter assembles are weighed:
        Balance Used:
        Weight Value:
       Balance Reads:
                First Weiahina
                                               Second Weiahina
                                                                       Third Weiahina
                                                                                    Average Weight
                                                                                    or Weight to be
                                                                                   Used as the Tare
                                                                                                . 2-7 T2,
                                                                                               1.27^3
                          <*.**> 2L
                                                                                       5/V3
      Balance Check after filter assemblies are weighed:
       Balance Reads:   	1
      COMMENTS:
      M5IFILTX.WPD June 4, 1998 Irev. M17FILT3.WPD November 5. 19991
24
                                                RCA#2 APPENDIX D

-------
                                FILTER ASSEMBLY TARE WEIGHT DATA
          MRI Project No.  104703.1.002.05.01
    Sampling Team Leader:  Jim Surman                         Analyst: _
      Filter Size and Type:  47mm diameter, Whatman QM-A quartz glass fiber filter
             Filter Lot No.  25460
   Assembly Components:  filter, aluminum foil gasket, and 316 stainless steel filter support
 Filter Assembly Treatment:  Heat at 105 °C for 3 hours, desiccate, and weigh to a constant weight.
             Weight Unit:  grams
          Date:
   Time Started:
Balance Check before filter assembies are weighed:
  Balance Used:
  Weight Value:
  Balance Reads:
                                                                                       Average Weight
                                                                                       or Weight to be
 Assembly No.        First Weighing         Second Weighing         Third Weighing         Used as the Tare
    ^\
    v
     •y	      "iffim/	       7, 'Witf	   	      'Z3?J-/7
                     , HI '1£>
    "A
Balance Check after filter assemblies are weighed:
 Balance Reads:      t^Tl""	        "<	
COMMENTS:                                                                            16
M5IFILTX.WPD June 4, 1998 (rev M17HLT3.WPD November 5. 1999)
                                                                                                      25
                                   RCA#2 APPENDIX D

-------
                                 RCA #2 Appendix E
                   M17 Post-Test Calibration Sheets
MRJ-OPPT\R4703-02-07 Appendices Covers WPD

-------
     METHOD 5 METERING CONSOLE CALIBRATION WITH CRITICAL ORIFICE
MR1 Project No.
Date:
Operator.

104703.1.002
11/21/99
D. Neal
Metering Console No.
=revious Dry Gas Meter Factor (Y):
Calibrated Critical Orifice No.
Critical Orifice Coefficient in English Units (K1):
| Ambient Temperature Meter No.
N11
1.010
D12
0.32080
Y-0783
CALIBRATION GAS VOLUME DATA
Initial Dry Gas Meter Gas Volume, ft.3
Final Dry Gas Meter Gas Volume, ft.3
Net Dry Gas Meter Gas Volume (Vm), ft.3
CALIBRATION CONDITIONS DATA
Dry Gas Meter Temperature, °F:
Initial Inlet Temperature, °F
Final Inlet Temperature, °F
Initial Outlet Temperature, °F
Final Outlet Temperature, °F
Average Dry Gas Meter Temperature (tj, °F
Time, seconds
Orifice Meter AH, inches H2O
Barometric Pressure, in. Hg
Critical Orifice Inlet (Ambient) Temperature, °F:
Initial Ambient Temperature, °F
Final Ambient Temperature, °F
Avg. Critical Orifice Inlet Temperature (tamb), °F
Pump Vacuum, in. Hg
COMPUTED CALIBRATION RESULTS
Critical Orifice Gas Volume (Vo.^)), standard ft.3
ry Gas Meter Gas Volume (Vm (ad)), standard ft.3
Dry Gas Meter Calibration Factor (Y)
Orifice Meter AH@
AVERAGE CALIBRATION RESULTS
Average Dry Gas Meter Calibration Factor (Y)
Average Orifice Meter AH@
CALIBRATION RESULTS COMPARISON
Criterion: Y Must Be Within 2% Of Average Y
Percent Difference Of Y From Average Y
Tolerance Result
COMPARISON WITH PRETEST RESULTS
Criterion: Y Must Be Within 5% Of Previous Y
% Difference Of Average Y From Previous Y
Tolerance Result
Run 1
269.601
273.772
4.171
76.0
77.0
74.0
75.0
75.5
600
0.540
30.01
69.0
70.0
69.5
18
4.185
4.130
1.013
1.720
1.013
1.717
0.01%
PASS
0.31%
PASS
Run 2
273.772
277.937
4.165
77.0
78.0
75.0
76.0
76.5
600
0.540
30.01
69.0
70.0
69.5
18
4.185
4.117
1.017
1.716
Run 3
277.937
282.137
4.200
78.0
79.0
76.0
77.0
77.5
600
0.540
30.01
70.0
70.0
70.0
18
4.183
4.143
1.010
1.715

0.34%
PASS
0.35%
PASS

Y = 1 013163954203880
  Remarks:
                                                               ft
CRORCALB.xls 10/29/99 (rev. N11CALB112199 11/21/99 10:51 AM)
                          RCA#2 APPENDIX E

-------
                  CONSOLE CALIBRATION WORKSHEET



Job No.   /OY703 . /• °0^	 Console No.     /I///

Date      //-<7L/*^f                 Orifice No.     2
Performed  By  /J.  /vffloo	 K Factor     0,32-0%

Barometer     5°» °)	 in. Hg.   Previous Y   -^r&£&- />oi	

NOTE:   Prior to running calibration,  connect mercury manometer
to sample  orifice.  Turn on  pump and bring mercury  manometer up
to 18.0 in.  Hg.    Record mercury manometer  and  console  vacuum
gauge  readings  below.   Insert   critical  orifice into  console
sample  orifice.    Set  console vacuum gauge at  18.0  in.  Hg. +/-
the console  vacuum gauge correction factor calculated  below.
 Mercury manometer  readings:  .A//*   +  fJ/x   =     18.0  In. Hg.

                Console  vacuum gauge reading:     A//O   In. Hg.

      Console vacuum  gauge  correction factor:     w//t   In. Hg.
                               RUN #1        RUN #2        RUN #3
 DGM Initial Volume-.         34f. fo/ **""*'•**
                     Initial: -341J-6+      ^73.771       £77,937

                       Final:   £7J.77>     277-9J7
 DGM Inlet Temperature:
                     Initial:    7£            77            7
-------
                  M5 CONSOLE POST TEST CHECKLIST
Job No.
                   /.
                                 Date
Console No.
                /V7/
                                  Performed By
Place  a  check (in  black ink)  in the  space provided after  the
required checks are performed.


 1.    \,   Perform positive leak  check  of  Delta H manometer.
            (See back of this sheet.)

 2.    \   Leak check Delta P manometer.

 3.    A/A1  Clean  pump.

 4.    \/   Clean  muffler jar(s) .

 5.    \   Inspect/refill oiler jar.
6. \, Calibrate DGM

Note: Reading must be
Within +/-5.4°F
thermocouples :

DGM Inlet:
DGM Outlet:
Reference
Thermometer*
°F
6 s.i
tf'l
                                                            DGM
                                                         Thermometer*
                                                             °F
  7.    \y   Digital clock/timer in place  and functional.

  8.    \   Vacuum check.  (Leak check  at  25  in.  Hg. vacuum. Leak
                           rate should be zero.)
       \	 Check indicator  lights.

       \,	 Check thermocouple switched.

        	 Check fan.

       Vy   Check pump  heater.

           Check heat  controllers.
       V
 9.

 10

 11

 12

 13

 14   	
If  any of  the  above items  were  replaced  or repaired,  please
document that  information below:
       V
            Check Orsat pump and  rotameter.
* Reference  Thermometer:
                                         Serial Number:
Calibration Records\Calibration Forms\M5check.doc
                                                          Revised 10/28/98
                          RCA#2 APPENDIX E

-------
Procedure for positive leak check Delta H manometer:

1.  Pump must  not be run prior  to  this  test.   Pump  needs  to be
    cool in  order to  get  an  accurate  reading.
2.  Pump pressure and vacuum lines  must  be  connected to console.
3.  Null  switch  on  console  must  be in  the  down position so
    solenoid valve  is  open  to  the  sampling  stream  as  it is
    during testing.
4.  Plug meter exhaust and  clamp  off bottom tube  from exhaust
    which goes  to the Orsat  pump.
5.  Plug sample orifice.
6.  Close main  flow control  valve.
7.  Open fine  control valve.
8.  Disconnect  right side  Delta H manometer tube  on  front of
    console.
9.  Blow  into  tubing until  manometer  reads  5 to  7  inches of
    water, and  clamp  off.
    There should  be no change in manometer  reading.
10.  Make certain  you remove plug  and clamp from  meter exhaust
    immediately after this  test to  avoid  damage  to  the  meter
    pump when pump is started up!
calibrec\m5check 03/09/98

                         RCA#2 APPENDIX E

-------
     METHOD 5 METERING CONSOLE CALIBRATION WITH CRITICAL ORIFICE
           CALIBRATION(S) PERFORMED INCORRECTLY - MUST BE REDONE!!!
MR1 Project No.
Date:
Operator

104703.1.002
11/21/99
D. Neal
Metering Console No.
Previous Dry Gas Meter Factor (Y):
Calibrated Critical Orifice No.
Critical Orifice Coefficient in English Units (K1):
| Ambient Temperature Meter No.
N12
0.996
D12
0.32080
Y-0783
CALIBRATION GAS VOLUME DATA
Initial Dry Gas Meter Gas Volume, ft.3
Final Dry Gas Meter Gas Volume, ft.3
Net Dry Gas Meter Gas Volume (Vm), ft.3
CALIBRATION CONDITIONS DATA
Dry Gas Meter Temperature, °F:
Initial Inlet Temperature, °F
Final Inlet Temperature, °F
Initial Outlet Temperature, °F
Final Outlet Temperature, °F
Average Dry Gas Meter Temperature (tm), °F
Time, seconds
Orifice Meter AH, inches H2O
Barometric Pressure, in. Hg
Critical Orifice Inlet (Ambient) Temperature, °F:
Initial Ambient Temperature, °F
Final Ambient Temperature, °F
Avg. Critical Orifice Inlet Temperature (tarTlt)), °F
Pump Vacuum, in. Hg
COMPUTED CALIBRATION RESULTS
;ritical Orifice Gas Volume (Vcr(std)), standard ft.3
ry Gas Meter Gas Volume (Vm (eta)), standard ft.3
Dry Gas Meter Calibration Factor (Y)
Orifice Meter AH@
AVERAGE CALIBRATION RESULTS
Average Dry Gas Meter Calibration Factor (Y)
Average Orifice Meter AH@
CALIBRATION RESULTS COMPARISON
Criterion: Y Must Be Within 2% Of Average Y
Percent Difference Of Y From Average Y
Tolerance Result
COMPARISON WITH PRETEST RESULTS
Criterion: Y Must Be Within 5% Of Previous Y
% Difference Of Average Y From Previous Y
Tolerance Result
Run 1
588.598
592.772
4.174
79.0
79.0
74.0
75.0
76.8
600
0.530
30.01
72.0
72.0
72.0
18
4.175
4.123
1.013
1.692
1.010
1.692
0.23%
PASS
1 .43%
PASS
Run 2
592.772
596.969
4.197
79.0
80.0
75.0
76.0
77.5
600
0.530
30.01
73.0
73.0
73.0
18
4.171
4.140
1.007
1.692
Run 3
596.969
601.160
4.191
"' ; '^-"'M-V;": 	 "•"•}.
81.0
81.0
77.0
77.0
79.0
600
0.530
30.01
74.0
74.0
74.0

4.167
4.123
1.011
1.691

0.28%
PASS
0.05%
PASS

Y = 1 010267285942600
	 	 	 -vi /I
  Remarks:
CRORCALB-xIs 10/29/99 (rev. N12CALB112199  11/21/99  10:58 AM)
                          RCA#2 APPENDIX E

-------
                      CONSOLE CALIBRATION WORKSHEET
    Job No.  /OY7f>3- /i g^P"	 Console No.

    Date     //-^/^ ??	 Orifice No.

    Performed By   ft. fJfoL	 K  Factor
    Barometer    3°'° / _ in.  Hg.    Previous Y   -/.&JQ-  &,o   =  _ 18 . 0  In.  Hg .

                    Console vacuum gauge reading:      /J/xt   In.  Hg.

          Console  vacuum gauge correction factor:     fJ*   In.  Hg.
                                  RUN #1        RUN  #2         RUN #3
    DGM  Initial Volume:
                        Initial:  SQS.W8
                          Final
    DGM Inlet Temperature :
                        Initial:    ?7            7^             gf

                          Final:    7?            gO             81
     DGM Outlet Temperature:
                        Initial:    ?y            7.f            77

                          Final:    if            li            11

     Time of run (  In Seconds  ) :    6oO           6^°           £oj
     Orifice Delta H  (in. H20) :    
-------
            METHOD 5 METERING CONSOLE CALIBRATION
                CRITICAL ORIFICE BRACKETING DATA
MRI Project No.
Date:
Operator
Metering Console No.
Dry Gas Meter Factor (Y):
Orifice Used for the Calibration:
Ambient Temperature Meter No.
104703.1.002
11/21/99
D. Neai
N12
1.010
D12
Y-0783
Note' Critical orifice coefficients are in English units.
|
Critical Orifice Being Evaluated
Critical Orifice No.
D12
Critical Orifices Used For Bracketing
First Orifice
Critical Orifice No.
Coefficient (K1):
Second Orifice
Critical Orifice No.
Coefficient (K1):
D16
0.44410
D19
0.51210
CALIBRATION GAS VOLUME DATA
Initial Dry Gas Meter Gas Volume, ft.3
Final Dry Gas Meter Gas Volume, ft.3
Net Dry Gas Meter Gas Volume (VJ, ft.3
CALIBRATION CONDITIONS DATA
Dry Gas Meter Temperature, °F:
Initial Inlet Temperature, °F
Final Inlet Temperature, °F
Initial Outlet Temperature, °F
Final Outlet Temperature, °F
Average Dry Gas Meter Temperature (tm), °F
Time, seconds
Orifice Meter AH, inches H2O
Barometric Pressure, in. Hg
Critical Orifice Inlet (Ambient) Temperature, °F:
Initial Ambient Temperature, °F
Final Ambient Temperature, °F
Average Critical Orifice Inlet Temperature (tamb), "F
Pump Vacuum, in. Hg
COMPUTED CALIBRATION RESULTS
Critical Orifice Gas Volume (Vor(sta)), standard ft.3
Dry Gas Meter Gas Volume (Vm (sts)), standard ft.3
Factor (Y) Obtained With Bracketing Orifice
CRITICAL ORIFICE ACCEPTABILITY
Criterion: All Ys Must Be Within 2% Of All Other Ys
Larger % Difference Between Dry Gas Meter Factor (Y)
And Factor (Y) Obtained With The Bracketing Orifice
Larger % Difference Between Factors (Ys)
Obtained With Bracketing Orifices
Acceptability Result
First Orifice
601.801
607.618
5.817
82.0
84.0
78.0
78.0
80.5
600
1.000
30.01
74.0
75.0
74.5
18
5.766
5.713
1.009
0.07%
0.29%
Second Orifice
607.901
614.637
6.736
84.0
86.0
79.0
79.0
82.0
600
1.400
30.01
75.0
75.0
75.0
18
6.646
6.604
1.006
0.36%


All Orifices Are Acceptable
Remarks:
CRORBRKT.xls 10/29/98 (rev. N12BRKT112199 11/21/99 11:03 AM)
                      RCA#2 APPENDIX E

-------
                      CONSOLE  BRACKETING WORKSHEET
    Job No.  /QYloj . /. oo2-	 Console No.      ///>•
    Date     //"-^'  _ Bracketing Orifice No . 1
    Performed By    • /l/» 6. _                K Factor   O ,
    Calibration Orifice No.  ^/>  Bracketing Orifice No. 2    2) /f

    New Y Factor 	                K Factor  __£	

    Barometer   1?°^ °'     in.  Hg.

    NOTE:    Prior  to running  calibration,  connect  mercury manometer
    to sample orifice.   Turn on pump  and bring mercury  manometer up
    to 18.0  in. Hg.   Record mercury  manometer and console  vacuum
    gauge  readings 'below.    Insert  critical  orifice  into  console
    sample orifice.   Set console vacuum  gauge at  18.0  in. Hg.  +/-
    the console vacuum gauge  correction factor calculated  below.


    Mercury manometer  readings:  A//*   +  A//C  =    18.0   in. Hg.

                   Console vacuum gauge reading:   - ;J/x>   in. Hg.

         Console vacuum gauge correction factor:    A///fl    in. Hg.
                                       RUN #1               RUN #2
     DGM Initial Volume:
                        Initial:     6°l
                          Final:      6o7. 6/8             6fif- 637
     DGM Inlet Temperature:
                        Initial -.
                          Final:       I?	     	S6_
     DGM Outlet Temperature:
                        Initial:
                          Final:       7g	     	7J_

     Time of run  ( In Seconds  ):       600                 600
     Orifice Delta H(in. H20) :         /, 0	          /•
     Room Temperature:
                         Initial:       7?                  7
                           Final:       75"
     Pump Vacuum  (in. Hg  ) :        _ 18 . 0 _      _ 18 . 0



    Calibration Records\Calibration Forms\conbrkws4d.doc   pty/temgrOs^ -ft ' •£. Y"f>lv^       Revised 02/03/99
O
                             RCA#2 APPENDIX E

-------
                  M5 CONSOLE POST TEST  CHECKLIST
 Job No.
                                  Date
Console No.
                 ///>-
                            Performed By
 Place  a  check  (in  black ink)  in the  space provided after  the
 required checks are performed.
 1.


 2.

 3.

 4.

 5.
\   Perform positive  leak  check of Delta H manometer.
     (See back of this  sheet.)

 V   Leak check Delta  P manometer.

tJ/A  Clean pump.

\   Clean muffler  jar(s).

     Inspect/refill  oiler jar.
       \,
6. \/ Calibrate DGM

Note: Reading must be
Within +/-5.4°F
thermocouples :

DGM Inlet:
DGM Outlet:
Reference
Thermometer*
°F
t$->
£ S.f
                                                             DGM
                                                         Thermometer*
  7.    \,    Digital clock/timer  in  place and functional.

  8.    \,    Vacuum check.  (Leak  check at 25 in. Hg. vacuum.  Leak
                           rate  should be zero.)

        V    Check indicator lights.
 9.

 10.

 11.

 12.

 13.

 14.  	
If  any of  the  above  items  were  replaced  or  repaired,  please
document that  information below:
       V   Check thermocouple  switched.

       V   Check fan.

       v   Check pump heater.

       *\*   Check heat controllers .
        y   Check Orsat pump  and  rotameter.
* Reference  Thermometer:
                                         Serial Number:   
-------
   Procedure  for  positive  leak  check Delta H manometer:

   1.   Pump must not be run  prior to this  test.   Pump  needs to be
        cool in order to get an accurate reading.
   2.   Pump pressure and vacuum lines must be connected to console.
   3.   Null  switch  on  console must  be  in the  down  position so
        solenoid  valve  is  open to  the  sampling  stream  as  it is
        during testing.
   4.   Plug meter exhaust and clamp  off bottom  tube  from  exhaust
        which goes to the Orsat pump.
   5.   Plug sample orifice.
   6.   Close main flow control valve.
   7.   Open fine control valve.
   8.   Disconnect right  side  Delta  H manometer  tube on  front of
        console.
   9.   Blow  into tubing  until manometer  reads  5  to 7  inches of
        water, and clamp off.
        There should be no change in manometer reading.
   10.  Make certain you remove plug  and clamp  from meter  exhaust
        immediately after  this test  to avoid  damage to  the meter
        pump when pump is started up?
    calibrcc\m5check  03/09/98

10
                             RCA#2 APPENDIX E

-------
              STACK THERMOCOUPLE CALIBRATION DATA FORM
Job No.

Date
                  . /. QQ >•
           //
Stack Thermocouple No.  J/
-------
                  STACK THERMOCOUPLE CALIBRATION DATA FORM
    Job No.   /of 763. ! .

    Date      //
         Stack Thermocouple No.   3/Sff

         Probe No.     13
    Performed By ^.
          Pyrometer No.
    Avg.  Stack Temp.(°F)   /BO
    Reference Instrument:   Hart Scientific Model No. 9100A,  Serial
       No.  84414  Dry-well, HDRC Handheld  Block A.   This instrument
       is calibrated in accordance with ITS-90 and  ANSI/NCSL  Z540-1
       Reference Instrument
          Temp. ( °F )
Pyrometer Temp.
Temp. Difference
Temp. Difference
                                                              O.
                            /QJ
                                   - o.
       (ref.  Temp., F  + 460) -  (pyro.  Temp.,  F + 460]
                    (ref.  Temp.,  F  + 460)
                                                           X 100 < 1.5%
   Calibration Records\Calibration Forms\STCHartdoc
                                                                  Revised 10/29/98
12
                               RCA#2 APPENDIX E

-------
           GOOSENECK THERMOCOUPLE CALIBRATION DATA FORM
Job No.

Date
                                 Pyrometer No.
                   A///
Reference Thermometer
                                                           ASTM
 Performed  By  &












Pyrometer Temp.
(°F)
68
68












Temp. Difference
Tolerance: +/- 2 °F
+ 0.^
o.c












Calibration Records\Calibration Forms\Gntccal.doc
                                                              Revised 10/28/98
                                                                          13
                           RCA#2 APPENDIX E

-------
              GOOSENECK THERMOCOUPLE CALIBRATION DATA  FORM
Job No.  _/'o0












Ref. Thermometer
Temperature (°F)
^^
"w^frt' t LS
67












Pyrometer Temp.
CF)
/r
^j'












Temp. DifTerence
Tolerance: +/- 2 °F
-Ag
-}<*>












   Calibration Records\Calibration Forms\Gntccal.doc
                                                                 Revised 10/28/98
14
                               RCA#2 APPENDK E

-------
                   Tvoe S Pitot Tube Inspection Data Form
Pitot Tube #:     (3       Date: /X^Aff     Performed By:


Probe #:       8 	
Pitot tube assembly level?


Pitot tube openings damaged?


a,   =  _0	  °
Y    =    0    °,   9   =


z = A sin Y   	Q


co = A sin 6         (?
                      (in),
Calibration required?


Comments:
                                       I/   Yes


                                      	Yes (explain below)
                                      A   =
                                                             (in)
                                   (in); (< 0.125 in)


                                   (in); (< 0.03125 in)
                                                    (in),  DT =   0,2%
                                 Yes      //      No
                                                                               No


                                                                               No
                                                                                 (in)
                                            A  Tube Axis	TT ~	-=^	
                                                      	(	£_^—
                                                                      ^  >*»
 Longitudinal
 Tube Axis —*• —
 0.48 CM < Dt < 0.95 CM
 (3/16 in.)     (3/8 in.)
 Transverse
 Tube Axis
 Transverse
 Tube Axis
 Calibration Records\CaIibration Forms\newpitotdoc


                                 RCA#2 APPENDIX E
                                                                                  01/18/99
                                                                                           /J
                                                                                           n/ul"
                                                                                                15

-------
                            Type S Pitot Tube Inspection Data Form
        Pitot Tube #:


        Probe #:
                           Date:


                           Job#:
Pitot tube assembly level?


Pitot tube openings damaged?
Pi   =  _6


Y    =  _


z = A sin Y


cp = A sin 8


PA =
                             6   =
                      Performed By:
                           6.0
        Calibration required?


        Comments:
                                                       Yes


                                                       Yes (explain below)
                                    (in)
         (in); (< 0.03125 in)
                                                              (in),
       Yes
                                                    No
                                             J/l
                                                                                  No


                                                                                  No
                                                         (in)
16
                            -Ik,
                                  A - Side Plane
                                                        Longitudinal    (,
                                                      A  Tube Axis — -,
                                                                            Ftowt
Longitudinal     r
 Tube Axis -*— f
                       |         	•!       Note:

                       DT       A     \X  l1^. f l.Q5Dt
-------
           ON SITE MERCURY BAROMETER READING CORRECTION
    AND AfccRQiiJ SAi\Gftr Tf» mperattire:       ;IH,I>H in Hg

                 Correction K>r GiriVfly:       -o,»X5 in. Hn

                    R«auiiiU Coiiufckrd FuJ tsfriviiy:       bO.uo  ui.
                             t 0. No.:

                             usinntnj;       30.tX> in. Hu

              «.«a«f»r**i«jf» «.J»w* kesuii'   wishin*' 1  IP. mi
                     After Auiusijnent:   _________   ui. i iq
                        RCA#2 APPENDIX E

-------
  GO
                                                    SAMPLING NOZZLE CALIBRATION CHECK DATA
                MRI Project No.  4702.02.04.09
                 Client/Source:  U.S. EPA OAQPS EMAD EMC / Cogentrix Unit 2A
               Source Location:  Rocky Mount, North Carolina
             Sampling Location:  Baghouse (Fabric Filter) Outlet  Duct
I
W
              Nozzle I.D. Number or
              Dedicated Sampling
                 Train Number
   Nozzle Type
(Shape and Material
 of Construction)
                                           n
                                           st
                                           t/
            COMMENTS:
Three Measured Diameters, inches
   D1         D2        D3
                                                            OJ92-
Average
Diameter,
 inches
                                                            ASM
Measured Bv
                                                                                                                                 Date
                                                                       a;fa   J.sPC,
            NOZZLCAX.WPD April 29, 1996 (lev. NOZZLCA1.WPO July 2, 1999)

-------
                                                       SAMPLING NOZZLE CALIBRATION CHECK DATA
                 MRI Project No. 104703.1.002.05.01
                   Client/Source: U.S. EPA OAQPS EMAD EMC / Cogentrix Unit 2A
                Source Location: Rocky Mount, North Carolina
              Sampling Location: Baghouse (Fabric Filter) Outlet Duct
               Nozzle I.D. Number or
                Dedicated Sampling
                  Train Number
   Nozzle Type
(Shape and Material
 of Construction)
Three Measured Diameters, inches
   D1          D2        D3
Average
Diameter,
 inches
I
K>
Measured Bv
Date
tr)
              COMMENTS:
              NOZZLCAX.WPD April 29, 1996 (rev NOZZLCA3.WPD November 1O, 1999)

-------
                               RCA #2 Appendix F
                      PM CEMS Data for Each Run
MRI-OPPT\R4703-0:-07 Appendices Covers WPD

-------
RCA #2 Testing - Run 30: High PM concentration
11/16/99 ESCP5B Durag 300-40 Durag F904K Moisture Temp.
Time raw mA raw ra mA raw mA % deg C
12:15
12:16
12:17
12:18
12:19
12:20
12:21
12:22
12:23
12:24
12:25
12:26
12:27
12:28
12:29
12:30
12:31
12:32
12:33
12:34
12:35
12:36
12:37
12:38
12:39
12:40
12:41
12:42
12:43
12:44
12:45
12:46
12:47
12:48
12:49
12:50
12:51
12:52
12:53
12:54
12:55
12:56
12:57
12:58
12:59
13:00
13:01
13:02
13:03
14.54
12.15
9.88
10.43
9.90
11.02
11.31
11.26
10.94
11.19
11.39
10.91
10.77
11.47
11.35
9.76
10.11
10.09
11.51
13.81
13.49
11.94
9.86
9.97
9.79
11.12
11.81
11.81
11.25
11.91
11.70
11.94
11.58
11.60
12.09
10.64
10.29
10.63
10.83
13.51
14.56
13.24
9.87
10.00
10.43
11.01
11.86
11.76
11.44
20.32 Moisture monitor not working properly
20.47 F904K not working properly
23.20
24.01
20.65
19.27
19.11
19.93
16.54
18.52
18.91
17.34
18.50
19.93
20.83
26.05
29.08
28.39
20.02
20.11
20.08
18.79
22.12
22.66
22.33
19.18
19.99
21.13
18.41
19.17
19.45
19.21
18.70
20.32
21.04
24.37
29.92
30.79
22.54
20.74
21.13
21.40
22.99
24.58
26.11
20.17
21.58
21.46
19.33
RCA#2 APPENDIX F

-------
13:04
13:05
13:06
13:07
13:08
13:09
13:10
13:11
13:12
13:13
13:14
13:15
13:16
13:17
13:18
13:19
13:20
13:21
13:22
13:23
13:24
13:25
13:26
13:27
13:28
13:29
13:30
13:31
13:32
13:33
13:34
13:35
13:36
13:37
13:38
13:39
13:40
13:41
13:42
13:43
13:44
13:45
13:46
13:47
13:48
13:50
13:51
13:52
13:52
13:53
13:54
13:55
11.61
11.91
11.71
11.85
11.39
11.75
10.72
10.22
11.37
11.15
13.45
13.91
14.47
10.45
9.96
10.84
10.70
11.59
11.70
11.79
11.48
11.74
12.46
11.58
11.32
11.50
11.75
9.78
10.82
10.67
11.62
13.52
13.69
11.01
10.00
10.67
10.55
11.69
11.82
12.72
10.84
11.46
11.96
11.92
11.15
12.21
10.09
10.16
10.32
10.60
12.59
14.26
18.12
18.44
19.16
17.98
20.11
20.08
21.91
27.91
27.55
24.82
18.94
20.53
20.74
21.22
23.92
25.36
20.86
21.55
20.35
20.65
17.64
18.38
19.29
17.56
19.14
19.48
21.73
28.33
28.69
27.25
17.44
19.87
20.62
19.36
23.17
24.46
22.12
20.38
20.50
21.34
18.00
19.09
19.41
18.34
18.85
20.23
25.36
28.45
28.30
27.52
17.98
21.43
RCA#2 APPENDIX F

-------
13:56
13:57
13:58
13:59
14:00
14:01
14:02
14:03
14:04
14:05
14:06
14:07
14.77
10.82
9.97
10.67
11.40
12.13
12.45
12.54
11.58
12.35
12.38
12.29
20.11
20.71
24.88
26.41
23.62
23.14
22.84
22.18
19.21
20.26
21.10
19.48
Average
Minimum
Maximum
Run 30
11.
49
9.76
14.

77

For P5B &
M17
Results
Train A
Train B
Average

300-40
mg/acm
27
22
25.

.9
.4
15

21.56 #DIV/0!
16.54 0.00
30.79 0.00

For RSD &
F904K
mg/dscm
40.8
33
36.9
Failed precision
#DIV/0!
0.00
0.00







test.
                                                        #DIV/0!
                                                         0.00
                                                         0.00
                                                                             #DIV/0!
                                                        Moisture
                                                           %
                                                          11.1
                                                           11
                                                         11.05
                                  RCA#2 APPENDIX F

-------
RCA #2 Testing - Run 31 : High PM concentration
11/16/99 ESCP5B Durag 300-40 Durag F904K Moisture Temp.
Time raw mA raw ra mA raw mA % deg C
15:20
15:21
15:22
15:23
15:24
15:25
15:26
15:27
15:28
15:29
15:30
15:31
15:32
15:33
15:34
15:35
15:36
15:37
15:38
15:39
15:40
15:41
15:42
15:43
15:44
15:45
15:46
15:47
15:48
15:49
15:50
15:51
15:52
15:53
15:54
15:55
15:56
15:57
15:58
15:59
16:00
16:01
16:02
16:03
16:04
16:05
16:06
16:07
16:08
10.91
10.12
11.60
12.05
12.06
11.90
11.92
11.95
11.92
11.78
12.38
12.56
9.98
10.39
11.32
12.13
14.43
14.65
12.08
9.93
10.89
9.95
10.87
11.54
11.21
11.58
11.75
12.71
12.98
11.47
12.22
12.34
11.18
10.45
11.12
11.41
13.77
14.82
14.07
10.16
10.58
10.88
10.85
11.74
11.94
12.28
11.47
11.58
11.71
27.10 Moisture monitor not working properly
23.53 F904K not working properly
21.40
21.37
22.15
19.45
19.16
19.72
18.98
19.69
20.53
20.80
26.35
29.50
28.90
18.64
20.29
20.71
21.28
22.87
24.73
23.17
20.65
20.62
20.71
19.09
19.57
21.19
22.09
19.06
21.31
22.36
25.27
33.34
32.50
26.20
20.11
21.67
23.35
21.94
25.09
26.89
21.67
21.04
21.61
20.77
18.53
19.21
20.44
RCA#2 APPENDIX F

-------
16:09
16:10
16:11
16:12
16:13
16:14
16:15
16:16
16:17
16:18
16:19
16:20
16:21
16:22
16:23
16:24
16:25
16:26
16:27
16:28
16:29
16:30
16:31
16:32
16:33
16:34
16:35
16:36
16:37
16:38
16:39
16:40
16:41
16:42
16:43
16:44
16:45
16:46
11.58
12.03
11.70
10.62
9.85
10.68
11.67
12.48
13.79
14.56
10.03
10.50
10.55
10.24
11.41
12.05
12.20
11.21
12.52
12.28
11.78
11.83
12.52
11.56
9.93
10.33
11.21
12.10
14.91
15.00
11.14
9.91
10.08
9.83
11.67
11.87
11.93
12.24
18.40
19.24
19.61
22.18
28.06
29.29
27.28
17.86
19.72
20.44
21.04
24.49
24.22
22.06
21.13
21.82
21.82
18.40
19.83
19.99
17.82
19.39
21.07
21.91
27.85
31.60
30.25
21.37
22.30
23.74
21.82
23.86
25.96
23.17
21.40
21.82
21.40
19.30
Average
Minimum
Maximum
11.69
9.83
15.00
22.41
17.82
33.34
#DIV/0!
 0.00
 0.00
#DIV/0!
 0.00
 0.00
#DIV/0!
 0.00
 0.00
                                                                             #DIV/0!
                                    RCA#2  APPENDIX F

-------
Run 31
For P5B &
M17 300-40
Results mg/acm
Train A
Train B
Average
25.4

25.4
Single point 16.1
For RSD &
F904K
mg/dscm
37.8

37.8
23.7

Moisture
%
12.2

12.2
11
                              RCA#2 APPENDIX F

-------
RCA #2 Testing - Run 32: Mid-high PM concentration
11/17/99 ESCP5B Durag 300-40 Durag F904K Moisture
Time raw mA raw ra mA raw mA %
8:54
8:55
8:56
8:57
8:58
8:59
9:00
9:01
9:02
9:03
9:04
9:05
9:06
9:07
9:08
9:09
9:10
9:11
9:12
9:13
9:14
9:15
9:16
9:17
9:18
9:19
9:20
9:21
9:22
9:23
9:24
9:25
9:26
9:27
9:28
9:29
9:30
9:31
9:32
9:33
9:34
9:35
9:36
9:37
9:38
9:39
9:40
9:41
9:42
9.30
9.82
10.07
9.88
10.08
10.08
10.24
10.68
9.47
10.10
10.10
8.97
8.65
9.03
9.74
10.67
11.26
13.48
8.50
8.46
8.83
8.78
9.55
9.86
9.68
9.44
9.61
10.08
10.18
10.29
10.02
9.91
9.02
8.85
9.48
10.88
11.82
11.86
8.94
8.92
9.06
8.81
9.84
9.84
9.96
9.45
10.44
10.86
10.22
20.95
17.38
17.41
17.72
15.32
15.50
16.62
16.95
15.00
17.02
17.29
19.33
24.19
23.95
20.74
15.18
17.26
17.49
16.57
18.78
19.46
15.87
16.68
16.53
16.42
13.89
14.49
15.32
14.16
16.62
16.89
18.28
23.23
23.26
24.37
15.38
16.90
17.34
16.14
19.24
19.72
18.94
18.24
17.69
18.30
15.19
16.34
17.02
15.75
F904K broken 10.62
10.74
10.38
10.40
10.44
10.92
10.92
10.80
10.56
10.98
10.98
10.86
10.74
10.50
10.50
10.86
10.86
10.86
10.74
10.62
10.26
10.26
10.50
10.62
10.50
10.38
10.53
10.68
10.31
10.62
10.62
10.74
10.50
10.62
10.62
10.50
10.38
10.50
10.50
10.38
10.50
10.50
10.62
10.74
10.62
10.62
10.74
10.62
10.26
Temp.
degC
82
82
82
83
84
84
84
84
84
82
82
82
82
82
82
82
82
82
82
82
82
82
82
82
82
82
83
84
84
82
82
82
82
82
82
82
82
82
82
82
82
82
82
82
82
82
82
82
82
RCA#2 APPENDIX F

-------
9:43
9:44
9:45
9:46
9:47
9:48
9:49
9:50
9:51
9:52
9:53
9:54
9:55
9:56
9:57
9:58
9:59
10:00
10:01
10:02
10:03
10:04
10:05
10:06
10:07
10:08
10:09
10:10
10:11
10:12
10:13
10:14
Average
Minimum
Maximum
Run 32

M17
Results
Train A
Train B
Average
Single point
9.62
10.04
10.62
8.90
9.88
9.71
10.40
12.47
12.65
10.53
8.97
9.55
9.44
10.17
10.46
11.42
10.47
11.20
11.19
10.85
10.32
10.14
11.22
9.65
9.02
9.53
9.99
12.07
12.11
11.39
8.62
9.36
10.06
8.46
13.48

For P5B &
300-40
mg/acm
19.1

19.1
11.9
16.88
17.57
17.68
23.11
25.18
26.29
16.08
18.64
18.97
17.86
21.73
22.48
22.06
18.56
19.15
20.14
18.20
18.23
17.75
17.49
17.52
18.74
19.99
24.04
26.02
24.94
20.05
18.17
18.78
18.90
19.00
20.98
18.64
13.89
26.29

For RSD &
F904K
mg/dscm
27.8

27.8
17.5
             10.50
             10.50
             10.50
             10.38
             10.38
             10.38
             10.38
             10.26
             10.26
             10.38
             10.62
             10.86
             10.74
             10.86
             11.10
             10.86
             10.74
             10.86
             10.74
             10.38
             10.50
             10.50
             10.38
             10.26
             10.26
             10.50
             10.38
             10.38
             10.50
             10.50
             10.38
             10.62
            10.57
            10.26
            11.10
  82
  82
  82
  82
  82
  82
  82
  82
  82
  82
  82
  82
  82
  82
  82
  82
  82
  82
  82
  82
  82
  82
  82
  82
  82
  82
  82
  82
  82
  82
  82
  82
82.20
82.00
84.00
180
                     Moisture
                        %
                       11.3

                       11.3

                       11.9
RCA#2 APPENDIX F

-------
RCA #2 Testing - Run 33: Mid-high PM concentration
11/17/99 ESCP5B Durag 300-40 Durag F904K Moisture
Time raw mA raw ra mA raw mA %
11:33
11:34
11:35
11:36
11:37
11:38
11:38
11:39
11:40
11:41
11:42
11:43
11:44
11:45
11:46
11:47
11:48
11:49
11:50
11:51
11:52
11:53
11:54
11:55
11:56
11:57
11:58
11:59
12:00
12:01
12:02
12:03
12:04
12:05
12:06
12:07
12:08
12:09
12:10
12:11
12:12
12:13
12:14
12:15
12:16
12:17
12:18
12:19
12:20
11.74
9.38
9.20
9.64
9.51
10.48
10.34
10.90
10.01
9.77
10.23
10.26
9.49
10.08
10.26
9.05
9.52
9.37
9.77
11.37
11.45
11.32
8.60
9.31
8.74
8.67
9.83
9.68
9.76
9.30
9.47
9.93
9.35
9.26
9.69
8.78
8.26
8.30
9.12
10.53
11.21
11.29
8.68
8.75
9.07
9.48
10.33
10.17
10.68
20.62
20.05
20.95
22.57
18.48
19.51
19.54
19.78
17.65
16.10
15.89
15.88
15.10
16.78
17.24
20.17
24.79
25.42
20.32
16.29
17.90
18.07
18.46
19.42
20.62
16.30
17.51
17.90
16.63
13.93
14.59
15.41
14.73
15.93
16.59
16.86
20.80
20.95
20.47
13.84
16.19
16.85
17.55
19.60
21.04
20.23
19.03
18.66
18.93
F904K broken 10.20
10.32
10.32
10.32
10.44
10.56
10.56
10.56
10.56
10.44
10.44
10.32
10.20
10.44
10.32
10.44
10.68
10.68
10.68
10.68
10.44
10.68
11.05
11.05
11.05
10.92
11.05
11.01
10.86
10.98
11.10
10.98
10.74
10.86
10.98
10.98
10.74
10.62
10.62
10.50
10.62
10.74
10.86
10.86
11.10
10.98
11.10
11.10
11.10
Temp.
degC
84
84
84
84
84
84
84
84
84
84
84
84
84
84
84
84
84
84
84
84
84
84
84
84
84
84
84
83
82
82
82
82
82
82
82
82
82
82
82
82
82
82
82
82
82
82
82
82
82
RCA#2 APPENDIX F

-------
         12:21       9.74       15.08                    11.10                 82
         12:22       10.03       15.91                    11.10                 82
         12:23       10.16       16.47                    11.23                 82
         12:24       9.78       14.59                    10.98                 82
         12:25       9.09       15.51                    10.98                 82
         12:26       9.36       16.44                    10.86                 82
         12:27       9.13       17.86                    10.85                 82
         12:28       8.00       21.67                    10.68                 80
         12:29       8.58       23.14                    10.68                 80
         12:30       8.82       23.23                    10.71                 81
         12:31       9.87       15.75                    10.62                 82
         12:32       11.34       17.07                    10.62                 82
         12:33       11.98       17.75                    10.74                 82
         12:34       9.15       17.38                    10.74                 82
         12:35       8.95       19.48                    10.62                 82
         12:36       8.71       20.20                    10.62                 82
         12:37       8.84       18.58                    10.38                 82
         12:38       9.86       18.00                    10.26                 82
         12:39       9.51       17.84                    10.65                 83
         12:40       9.92       17.62                    10.80                 84
         12:41       9.36       14.50                    10.92                 84
         12:42       9.46       14.71                    11.05                 84
         12:43       9.59       15.10                    11.01                 83
         12:44       9.43       14.44                    10.86                 82
         12:45       8.86       14.34                    10.74                 82
         12:46       9.28       16.51                    10.86                 82
         12:47       9.46       16.75                    10.86                 82
         12:48       8.40       20.26                    10.74                 82
         12:49       8.44       22.24                    10.62                 82
         12:50       8.92       24.82                    10.62                 82
         12:51       9.12       15.93                    10.62                 82
         12:52       10.88       15.27                    10.50                 82
         12:53       10.90       15.70                    10.50                 82
         12:54       9.46       16.18                    10.50                 82
         12:55       8.58       16.73                    10.38                 82
         12:56       8.68       18.41                    10.50                 82
         12:57       8.64,       19.21                    10.43                 84
         12:58       9.02       16.29                    10.56                 84
         12:59       9.67       17.16                    10.56                 84
         13:00       9.93       17.65                    10.56                 84
         13:01       9.37       16.03                    10.80                 84
         13:02       10.01       16.18                    10.64                 83
         13:03       10.10       16.05                    11.05                 84
         13:04       10.13       16.49                    10.92                 84
         13:05       9.45       13.64                    10.56                 84
         13:06       9.64       14.80                    10.68                 84
         13:07       9.14       15.34                    10.68                 84
         13:08       8.69       17.68                    10.56                 84
         13:09       7.85       20.05                    10.20                 84
         13:10       8.21        20.23                    10.07                 84
         13:11       8.88       17.57                    9.95                  84
         13:12       9.75       13.67                    9.83                  84
10
                                           RCA#2 APPENDIX F

-------
13:13
13:14
13:15
13:16
13:17
13:18
13:19
13:20
13:21
13:22
13:23
13:24
10.57
11.79
8.19
8.46
9.08
8.92
9.96
10.26
10.11
9.95
10.28
10.31
15.09
17.12
15.52
19.72
20.44
17.59
18.87
18.85
18.15
15.53
15.87
16.33
                                                9.95
                                                10.07
                                                10.32
                                                10.32
                                                10.44
                                                10.20
                                                10.56
                                                10.70
                                                10.50
                                                10.50
                                                10.62
                                                10.74
                                                        84
                                                        84
                                                        84
                                                        84
                                                        84
                                                        84
                                                        84
                                                        85
                                                        86
                                                        86
                                                        86
                                                        86
Average
Minimum
Maximum

Run 33
 9.60
 7.85
11.98
17.77
13.64
25.42
10.66
9.83
11.23
83.05
80.00
86.00
181
For P5B &
M17 300-40
Results mg/acm
Train A
Train B
Average
19.2
17.7
18.45
For RSD &
F904K
mg/dscm
28.3
26
27.15
                                                        Moisture

                                                          12^3
                                                          11.6
                                                          11.95
                                   RCA#2 APPENDIX F
                                                                                               11

-------
RCA #2 Testing - Run 34: Medium-high PM concentration
11/17/99 ESCP5B Durag 300-40 Durag F904K Moisture
Time raw mA raw ra mA raw mA %
14:50
14:51
14:52
14:53
14:54
14:55
14:56
14:57
14:58
14:59
15:00
15:01
15:02
15:03
15:04
15:05
15:06
15:07
15:08
15:09
15:10
15:11
15:12
15:13
15:14
15:15
15:16
15:17
15:18
15:19
15:20
15:21
15:22
15:23
15:24
15:25
15:26
15:27
15:28
15:29
15:30
15:31
15:32
15:33
15:34
15:35
15:36
15:37
15:38
8.89
9.50
9.06
10.47
11.56
11.48
9.13
8.99
9.05
9.19
10.21
10.50
10.78
9.45
9.74
9.69
9.83
9.52
9.72
10.04
8.20
8.42
8.41
9.67
11.30
11.29
9.54
8.50
8.55
8.24
8.86
9.14
9.44
8.72
9.05
9.61
9.52
9.38
9.39
9.45
8.70
8.56
9.42
8.93
10.72
10.86
10.76
8.17
8.60
23.29
23.89
25.51
14.85
17.75
17.07
17.26
20.86
22.57
20.74
19.93
20.80
20.23
16.22
15.42
15.39
15.08
15.26
15.53
16.04
19.15
21.46
21.64
15.65
15.51
16.00
16.24
17.82
18.47
18.25
15.60
16.28
15.99
13.73
13.64
14.45
14.66
13.47
15.28
15.75
17.20
22.42
21.67
18.52
15.37
16.11
17.16
16.59
18.70
F904K broken 10.80
10.80
10.80
10.80
10.80
10.56
10.68
10.80
10.80
10.80
10.80
10.80
10.80
10.56
10.68
10.68
10.44
10.44
10.56
10.44
10.56
10.56
10.68
10.56
10.56
10.68
10.68
10.56
10.68
10.68
10.68
10.68
10.68
10.68
10.68
10.68
10.56
10.44
10.68
10.80
10.80
10.68
10.80
10.68
10.68
10.56
10.56
10.68
10.68
Temp.
degC
84
84
84
84
84
84
84
84
84
84
84
84
84
84
84
84
84
84
84
84
84
84
84
84
84
84
84
84
84
84
84
84
84
84
84
84
84
84
84
84
84
84
84
84
84
84
84
84
84
12
                                  RCA#2 APPENDIX F

-------
15:39
15:40
15:41
15:42
15:43
15:44
15:45
15:46
15:47
15:48
15:49
15:50
15:51
15:52
15:53
15:54
15:55
15:56
15:57
15:58
15:59
16:00
16:01
16:02
16:03
16:04
16:05
16:06
16:07
16:08
16:09
16:10
16:11
16:12
16:13
16:14
16:15

Average
Minimum
Maximum
8.56
8.71
9.16
9.50
9.55
9.60
9.81
9.98
9.74
9.83
9.98
8.87
8.57
9.17
8.78
10.40
11.03
11.67
8.17
8.47
8.30
8.50
9.02
9.70
9.79
8.92
9.43
9.51
9.52
8.89
9.07
8.84
7.95
8.31
8.57
9.12
10.71
P5B
9.42
7.95
11.67
  18.77
  15.61
  16.14
  16.66
  17.07
  14.54
  15.25
  15.93
  14.74
  16.05
  16.43
  18.07
  22.24
  23.65
  21.49
  14.65
  16.56
  16.88
  16.48
  18.14
  18.97
  16.75
  15.97
  16.93
  16.43
  13.40
  14.08
  14.90
  13.79
  14.57
  15.21
  15.56
  19.69
  20.89
  21.13
  14.06
  15.69

DR 300-40

  17.32
  13.40
  25.51
F904K
 10.56
 10.20
 10.56
 11.05
 10.92
 10.92
 11.05
 11.05
 10.79
 10.74
 10.74
 10.74
 10.67
 10.80
 10.80
 10.68
 10.80
 10.80
 10.68
 10.68
 10.68
 10.56
 10.68
 10.56
 10.44
 10.32
 10.44
 10.56
 10.32
 10.68
 10.80
 10.92
 10.77
 10.74
 10.74
 10.62
 10.62

Moisture

 10.68
 10.20
 11.05
 84
 84
 84
 84
 84
 84
 84
 84
 84
 82
 82
 82
 84
 84
 84
 84
 84
 84
 84
 84
 84
 84
 84
 84
 84
 84
 84
 84
 84
 84
 84
 84
 83
 82
 82
 82
 82

Temp

83.83
82.00
84.00
                                           183
              RCA#2 APPENDIX F
                                                                            13

-------
     Run 34
For P5B &
M17 300-40
Results mg/acm
Train A
Train B
Average
10.3

10.3
Single point 11.3
For RSD &
F904K
mg/dscm
15.3

15.3
16.7

Moisture
%
13

13
12.5
14
                                  RCA#2 APPENDIX F

-------
RCA #2 Testing - Run 35: Medium PM concentration
 11/18/99  ESCP5B Durag 300-40 Durag F904K  Moisture             Temp.
                                                               degC
                                                                84
                                                                84
                                                                84
                                                                84
                                                                84
                                                                84
                                                                84
                                                                84
                                                                84
                                                                84
                                                                84
                                                                84
                                                                84
                                                                84
                                                                84
                                                                84
                                                                84
                                                                84
                                                                84
                                                                84
                                                                84
                                                                84
                                                                84
                                                                84
                                                                84
                                                                84
                                                                84
                                                                84
                                                                84
                                                                84
                                                                84
                                                                84
                                                                84
                                                                84
                                                                84
                                                                84
                                                                84
                                                                84
                                                                84
                                                                84
                                                                84
                                                                84
                                                                84
                                                                 84
                                                                 84
                                                                 84
                                                                 84
                                                                 84
                                                                 84
Time
8:52
8:53
8:54
8:55
8:56
8:57
8:58
8:59
9:00
9:01
9:02
9:03
9:04
9:05
9:06
9:07
9:08
9:09
9:10
9:11
9:12
9:13
9:14
9:15
9:16
9:17
9:18
9:19
9:20
9:21
9:22
9:23
9:24
9:25
9:26
9:27
9:28
9:29
9:30
9:31
9:32
9:33
9:34
9:35
9:36
9:37
9:38
9:39
9:40
raw mA
7.31
7.51
8.01
8.16
7.42
7.70
7.92
7.91
7.56
7.45
7.65
7.18
7.25
7.20
7.20
8.10
8.58
8.53
6.77
6.94
6.98
7.21
7.53
7.72
7.79
7.25
7.74
7.79
7.65
7.66
7.67
7.71
7.17
7.37
7.44
8.45
9.10
9.32
7.56
7.23
7.55
7.83
7.98
8.24
8.43
7.82
8.24
8.41
8.46
raw ra mA
14.08
11.57
12.25
12.36
10.93
10.31
10.62
10.93
10.03
10.55
10.87
12.05
15.23
15.35
13.57
10.27
11.50
11.24
11.23
12.97
13.68
11.67
11.86
12.17
11.65
9.70
10.33
10.65
10.46
10.69
11.31
12.19
15.57
16.49
17.03
11.06
12.36
12.28
12.18
14.27
15.73
14.23
12.89
13.66
13.39
11.90
12.18
12.20
12.35
raw mA











7.05
7.05
7.05
7.05
7.05
7.05
7.05
7.05
7.05
7.05
7.05
7.05
7.05
6.82
6.82
6.82
6.82
6.82
6.82
6.82
6.82
6.82
6.82
6.82
6.82
6.82
6.58
6.50
6.50
6.50
6.50
6.50
6.50
6.50
6.50
6.50
6.50
6.50
%
10.68
10.80
10.80
10.80
10.68
10.80
10.80
10.80
10.32
10.68
10.68
10.68
10.68
10.68
10.68
10.56
10.68
10.68
10.68
10.68
10.80
10.80
10.92
10.92
10.80
10.80
10.92
10.80
10.32
10.56
10.56
10.68
10.80
10.80
10.80
10.68
10.80
10.80
10.80
10.68
10.68
10.68
10.68
10.68
10.68
10.44
10.68
10.68
10.32
                                                                                          15
                                  RCA#2 APPENDIX F

-------
9:41
9:42
9:43
9:44
9:45
9:46
9:47
9:48
9:49
9:50
9:51
9:52
9:53
9:54
9:55
9:56
9:57
9:58
9:59
10:00
10:01
10:02
10:03
10:04
10:05
10:06
10:07
10:08
10:09
10:10
10:11
10:12
10:13
10:14
10:15
10:16
10:17
10:18
10:19
10:20
10:21
10:22
10:23
10:24
10:25
10:26
10:27
10:28
8.14
8.44
8.69
7.63
7.71
7.65
8.43
9.44
9.58
8.46
7.30
7.38
8.15
8.06
8.30
8.35
7.77
8.27
8.40
8.40
8.03
8.16
8.44
7.88
7.98
7.54
7.79
9.17
9.53
9.38
7.57
8.15
8.43















12.49
13.78
14.08
17.85
19.39
18.88
13.73
13.57
13.64
13.46
14.92
15.64
15.91
13.33
14.11
14.35
12.44
11.91
12.70
12.78
12.44
13.26
13.82
14.83
18.35
18.57
14.76
13.03
13.41
14.68
15.60
17.25
18.36















6.50
6.97
7.13
7.13
7.13
7.13
7.13
7.13
7.13
7.13
7.13
7.13
7.13
7.13
6.98
6.82
6.82
6.82
6.82
6.82
6.82
6.82
6.82
6.82
6.82
6.82
6.82
6.96
7.38
7.38
7.38
7.38
7.38
7.38
7.38
7.38
7.38
7.38
7.38
7.38
7.38
9.21
9.21
9.21
9.21
9.21
9.21
9.21
10.68
10.80
10.80
10.80
10.80
10.80
10.68
10.68
10.80
10.80
10.68
10.68
10.56
10.68
10.68
10.68
10.56
10.68
10.68
10.44
10.56
10.68
10.68
10.68
10.68
10.68
10.56
10.56
10.68
10.68
10.80
10.80
10.68















                                                                     84
                                                                     84
                                                                     84
                                                                     84
                                                                     84
                                                                     84
                                                                     84
                                                                     84
                                                                     84
                                                                     84
                                                                     84
                                                                     84
                                                                     84
                                                                     84
                                                                     84
                                                                     84
                                                                     84
                                                                     84
                                                                     84
                                                                     84
                                                                     84
                                                                     84
                                                                     84
                                                                     84
                                                                     84
                                                                     84
                                                                     84
                                                                     84
                                                                     84
                                                                     84
                                                                     84
                                                                     84
                                                                     84
16
                                      RCA#2 APPENDIX F

-------
Average
Minimum
Maximum

Run 35
P5B

7.95
6.77
9.58
DR 300-40

  13.31
  9.70
  19.39
F904K

 7.14
 6.50
 9.21
Moisture

 10.70
 10.32
 10.92
Temp

84.00
84.00
84.00
183
For P5B &
M17 300-40
Results mg/acm
Train A
Train B
Average
13.6

13.6
Single point 7.7
For BSD &
F904K
mg/dscm
19.7

19.7
11.2
                                                       Moisture
                                                          %
                                                          12

                                                          12

                                                         11.4
                                  RCA#2 APPENDIX F
                                                                                             17

-------
     RCA #2 Testing - Run 36: Mid-high PM concentration
                                                                    Temp.
                                                                    degC
                                                                      84
                                                                      84
                                                                      84
                                                                      84
                                                                      84
                                                                      84
                                                                      84
                                                                      84
                                                                      84
                                                                      84
                                                                      84
                                                                      84
                                                                      84
                                                                      84
                                                                      84
                                                                      84
                                                                      84
                                                                      84
                                                                      84
                                                                      84
                                                                      84
                                                                      84
                                                                      84
                                                                      84
                                                                      84
                                                                      84
                                                                      84
                                                                      84
                                                                      84
                                                                      84
                                                                      84
                                                                      84
                                                                      84
                                                                      84
                                                                      84
                                                                      84
                                                                      84
                                                                      84
                                                                      84
                                                                      84
                                                                      84
                                                                      84
                                                                      84
                                                                      84
                                                                      84
                                                                      84
                                                                      84
                                                                      84
                                                                      84
11/18/99
Time
11:05
11:06
11:07
11:08
11:09
11:10
11:11
11:12
11:13
11:14
11:15
11:16
11:17
11:18
11:19
11:20
11:21
11:22
11:23
11:24
11:25
11:26
11:27
11:28
11:29
11:30
11:31
11:32
11:33
11:34
11:35
11:36
11:37
11:38
11:39
11:40
11:41
11:42
11:43
11:44
11:45
11:46
11:47
11:48
11:49
11:50
11:51
11:52
11:53
ESC P5B
raw mA
10.23
10.82
11.60
12.08
13.58
13.88
12.00
10.51
10.72
11.13
11.54
12.04
12.68
12.21
12.46
12.88
13.00
11.94
12.33
11.98
11.28
10.41
10.23
10.79
12.69
12.84
12.30
9.38
9.13
10.26
9.75
10.99
11.08
11.20
11.02
11.21
11.26
11.52
10.50
10.32
10.23
9.26
9.17
9.72
10.64
12.33
12.68
8.89
9.01
Durag 300-40
raw ra mA
29.80
33.52
33.28
23.11
22.63
23.11
24.04
25.78
30.16
29.95
24.85
25.81
25.09
23.26
22.06
23.35
24.46
22.06
23.80
25.33
26.08
33.13
32.23
26.77
21.67
23.26
23.20
21.16
24.85
25.51
20.47
22.27
21.31
21.01
18.83
18.81
19.03
18.15
18.64
20.41
22.60
26.05
26.47
26.29
17.11
19.63
20.29
20.23
21.97
Durag F904K
raw mA










10.65
10.65
10.65
10.65
10.65
10.65
10.65
10.65
10.65
10.65
10.65
10.65
10.65
11.25
11.45
11.45
11.45
11.45
11.45
11.45
11.45
11.45
11.45
11.45
11.45
11.45
10.45
9.45
9.45
9.45
9.45
9.45
9.45
9.45
9.45
9.45
9.45
9.45
9.45
Moistur
%
10.44
10.32
10.32
10.20
10.20
10.32
10.44
10.44
10.68
10.68
10.68
10.56
10.68
10.56
10.56
10.56
10.56
10.20
10.32
10.32
10.32
10.20
10.20
10.20
10.20
10.20
10.20
10.20
10.20
10.20
10.07
10.20
10.20
10.07
10.20
10.20
10.20
9.95
10.20
10.32
10.44
10.32
10.44
10.32
10.32
10.32
10.32
10.32
10.44
18
                                      RCA#2 APPENDIX F

-------
11:54
11:55
11:56
11:57
11:58
11:59
12:00
12:01
12:02
12:03
12:04
12:05
12:06
12:07
12:08
12:09
12:10
12:11
12:12
12:13
12:14
12:15
12:16
12:17
12:18
12:19
12:20
12:21
12:22
12:23
12:24
12:25
12:26
12:27
12:28
12:29
12:30
12:31
12:32
12:33
9.29
9.44
10.64
10.98
11.28
10.58
11.45
11.71
11.31
10.67
10.91
10.42
9.50
9.68
9.96
10.38
12.21
13.53
12.06
9.31
9.52
9.13
10.73
10.44
11.10
10.03
10.71
11.00
11.27
10.45
11.00
10.89








23.11
20.50
20.68
22.09
22.06
17.58
19.32
19.99
18.07
19.44
20.41
20.74
25.69
28.81
28.03
17.51
19.54
20.95
20.26
22.78
24.25
22.93
20.74
20.77
21.10
16.77
17.44
18.25
18.40
18.73
20.29
20.50








9.73
10.01
10.01
10.01
10.01
10.01
10.01
10.01
10.01
10.01
10.01
10.01
10.01
10.07
10.25
10.25
10.25
10.25
10.25
10.25
10.25
10.25
10.25
10.25
10.25
10.25
10.25
9.85
9.85
9.85
9.85
9.85
9.85
9.85
9.85
9.85
9.85
9.85
9.85
9.85
10.44
10.20
10.44
10.68
10.68
10.68
10.80
10.80
10.56
10.50
10.74
10.74
10.74
10.74
10.86
10.62
10.38
10.50
10.74
10.74
10.86
10.62
10.74
10.74
10.62
10.38
10.50
10.62
10.50
10.74
10.74
10.98








Average
Minimum
Maximum
 P5B

11.00
 8.89
13.88
DR 300-40

  22.72
  16.77
  33.52
F904K

10.28
 9.45
11.45
Moisture

 10.45
  9.95
 10.98
                                                                   84
                                                                   84
                                                                   84
                                                                   84
                                                                   84
                                                                   84
                                                                   84
                                                                   84
                                                                   84
                                                                   82
                                                                   82
                                                                   82
                                                                   82
                                                                   82
                                                                   82
                                                                   82
                                                                   82
                                                                   82
                                                                   82
                                                                   82
                                                                   82
                                                                   82
                                                                   82
                                                                   82
                                                                   82
                                                                   82
                                                                   82
                                                                   82
                                                                   82
                                                                   82
                                                                   82
                                                                   82
Temp

83.43
82.00
84.00
182
                                  RCA#2 APPENDIX F
                                                                                             19

-------
     Run 36
For P5B &
M17 300-40
Results mg/acm
Train A
Train B
Average
26.6

26.6
Single point 15.3
For RSD &
F904K
mg/dscm
38.5

38.5
22.6

Moisture
%
11.6

11.6
12.5
20
                                   RCA#2 APPENDIX F

-------
RCA #2 Testing - Run 37: High PM concentration
 11/18-19/99  ESC P5B Durag 300-40 Durag F904K  Moisture             Temp.
                                                                degC
                                                                 84
                                                                 84
                                                                 84
                                                                 83
                                                                 82
                                                                 82
                                                                 82
                                                                 82
                                                                 82
                                                                 82
                                                                 82
                                                                 82
                                                                 82
                                                                 82
                                                                 82
                                                                 82
                                                                 82
                                                                 82
                                                                 82
                                                                 82
                                                                 82
                                                                 82
                                                                 82
                                                                 82
                                                                 82
                                                                 82
                                                                 82
                                                                 82
                                                                 82
                                                                 82
                                                                 82
                                                                 82
                                                                 82
                                                                 82
                                                                 82
                                                                 82
                                                                 82
                                                                 82
                                                                 82
                                                                 82
                                                                 82
                                                                 82
                                                                 82
                                                                 82
                                                                 82
                                                                 82
                                                                 82
                                                                 82
                                                                 82
Time
23:24
23:25
23:26
23:27
23:28
23:29
23:30
23:31
23:32
23:33
23:34
23:35
23:36
23:37
23:38
23:39
23:40
23:41
23:42
23:43
23:44
23:45
23:46
23:47
23:48
23:49
23:50
23:51
23:52
23:53
23:54
23:55
23:56
23:57
23:58
23:59
0:02
0:03
0:04
0:05
0:06
0:07
0:08
0:09
0:10
0:11
0:12
0:13
0:14
raw mA
12.94
15.14
15.49
14.68
12.84
11.66
14.58
14.60
14.40
13.70
15.18
14.17
13.95
12.47
13.72
13.74
14.32
16.07
15.86
13.05
12.68
12.68
11.89
14.20
14.69
14.25
12.14
12.10
12.25
13.64
12.75
13.43
12.94
14.41
14.20
14.88
14.36
11.82
12.68
12.94
12.31
15.04
15.03
14.69
11.52
12.20
12.24
11.76
13.40
raw ra mA
22.75
25.72
26.62
25.48
20.02
19.90
24.31
26.86
27.22
23.65
24.19
24.61
25.84
30.40
32.32
31.24
20.89
23.14
23.38
24.94
29.89
30.40
25.75
22.42
23.29
23.53
18.88
19.90
19.18
19.48
19.55
18.61
19.48
25.33
25.93
26.74
25.42
23.98
29.83
31.03
26.17
21.40
21.97
21.52
23.74
27.31
27.70
19.93
21.61
raw mA











14.89
14.89
14.89
14.89
14.89
14.89
14.89
14.89
14.89
14.89
14.89
14.89
14.89
15.13
15.21
15.21
15.21
15.21
15.21
15.21
15.21
15.21
15.21
15.21
15.21
13.84
13.84
13.84
13.84
13.84
13.84
13.84
13.84
13.84
13.84
13.84
13.84
14.10
%
8.98
9.22
9.22
9.19
9.17
9.05
9.05
9.17
9.05
8.93
9.05
9.29
9.17
9.05
9.05
8.93
9.17
9.29
9.29
9.17
9.17
9.29
9.17
9.17
9.17
9.29
9.05
9.17
9.17
9.05
8.81
9.17
9.29
9.66
9.41
9.17
9.17
9.17
9.17
9.17
9.05
9.05
9.05
9.05
9.05
9.05
9.05
9.05
9.17
                                                                                           21
                                 RCA#2 APPENDIX F

-------
0:15
0:16
0:17
0:18
0:19
0:20
0:21
0:22
0:23
0:24
0:25
0:26
0:27
0:28
0:29
0:30
0:31
0:32
0:33
0:34
0:35
0:36
0:37
0:38
0:39
0:40
0:41
0:42
0:43
0:44
0:45
0:46
0:47
0:48
0:49
0:50
0:51
0:52
0:53
13.19
12.79
12.29
11.27
10.98
12.17
11.39
12.87
13.09
13.43
14.10
13.67
13.68
14.46
14.80
13.38
12.25
14.21
14.43
15.62
15.86
14.08
12.08
12.66
11.83
13.13
13.38
14.01
13.59
11.49









20.62
20.35
17.71
17.96
16.44
17.22
18.24
17.33
19.42
24.31
25.12
23.41
22.24
24.94
25.06
26.38
30.67
30.49
23.23
22.27
23.02
21.37
27.61
29.02
26.53
21.52
23.02
21.82
21.04
19.63









14.89
14.89
14.89
14.89
14.89
14.89
14.89
14.89
14.89
14.89
14.89
14.89
14.89
14.41
14.41
14.41
14.41
14.41
14.41
14.41
14.41
14.41
14.41
14.41
14.41
14.41
15.31
15.61
15.61
15.61
15.61
15.61
15.61
15.61
15.61
15.61
15.61
15.61
15.61
9.05
8.81
8.93
9.05
9.05
9.05
8.81
9.17
9.29
9.17
9.17
8.93
9.05
9.05
8.93
9.05
9.17
9.05
9.05
9.17
9.17
9.17
9.05
9.17
9.17
9.17
9.29
9.29
9.05
8.93









     Average
     Minimum
     Maximum
 P5B

13.44
10.98
16.07
DR 300-40

  23.69
  16.44
  32.32
F904K

14.80
13.84
15.61
Moisture

  9.12
  8.81
  9.66
                                                                         82
                                                                         82
                                                                         82
                                                                         82
                                                                         82
                                                                         82
                                                                         82
                                                                         82
                                                                         82
                                                                         82
                                                                         82
                                                                         82
                                                                         82
                                                                         82
                                                                         82
                                                                         82
                                                                         82
                                                                         82
                                                                         82
                                                                         82
                                                                         82
                                                                         82
                                                                         82
                                                                         82
                                                                         82
                                                                         82
                                                                         82
                                                                         82
                                                                         82
                                                                         82
Temp

82.09
82.00
84.00
180
22
                                        RCA#2 APPENDIX F

-------
Run 37
For P5B &
M17 300-40
Results mg/acm
Train A
Train B
Average
57.6

57.6
Single point 36.8
For RSD &
F904K
mg/dscm
80.2

80.2
51.1

Moisture
%
10.5

10.5
9.8
                             RCA#2 APPENDIX F
                                                                                23

-------
     RCA#2 Testing - Run 38: Mid-high PM concentration
      11/19/99   ESCP5B  Durag 300-40 Durag F904K  Moisture             Temp.
                                                                     deg C
                                                                      82
                                                                      82
                                                                      82
                                                                      82
                                                                      82
                                                                      82
                                                                      82
                                                                      82
                                                                      82
                                                                      82
                                                                      82
                                                                      82
                                                                      82
                                                                      82
                                                                      82
                                                                      82
                                                                      82
                                                                      82
                                                                      82
                                                                      82
                                                                      82
                                                                      82
                                                                      82
                                                                      82
                                                                      82
                                                                      82
                                                                      82
                                                                      82
                                                                      82
                                                                      82
                                                                      82
                                                                      82
                                                                      82
                                                                      82
                                                                      82
                                                                      82
                                                                      82
                                                                      82
                                                                      82
                                                                      82
                                                                      83
                                                                      84
                                                                      84
                                                                      84
                                                                      84
                                                                      83
                                                                      82
                                                                      82
                                                                      82
Time
1:37
1:38
1:39
1:40
1:41
1:42
1:43
1:44
1:45
1:46
1:47
1:48
1:49
1:50
1:51
1:52
1:53
1:54
1:55
1:56
1:57
1:58
1:59
2:00
2:01
2:02
2:03
2:04
2:05
2:06
2:07
2:08
2:09
2:10
2:11
2:12
2:13
2:14
2:15
2:16
2:17
2:18
2:19
2:20
2:21
2:22
2:23
2:24
2:25
raw mA
8.83
9.38
9.81
9.87
10.59
10.64
11.00
9.39
9.49
9.47
9.18
8.93
9.99
9.74
9.85
10.05
10.01
10.47
10.55
10.36
11.75
11.32
10.79
11.61
11.24
12.11
10.09
10.67
10.58
11.61
12.15
12.49
11.04
9.66
9.98
10.06
10.33
10.69
11.93
10.39
9.59
9.83
9.94
10.34
9.71
10.16
9.69
9.87
10.48
raw ra mA
18.35
20.80
20.83
15.11
15.00
16.03
16.18
13.44
13.51
13.96
14.30
14.09
15.01
14.38
13.72
14.57
14.35
13.84
14.76
16.96
19.57
20.50
18.37
19.96
19.69
20.05
21.91
23.41
23.20
15.94
17.39
16.96
16.18
20.05
21.16
20.05
15.59
15.29
17.12
15.54
14.09
14.28
14.44
15.05
14.73
14.07
14.80
15.03
14.52
raw mA











11.21
11.21
11.21
11.21
11.21
11.21
11.21
11.21
11.21
11.21
11.21
11.21
11.41
11.61
11.61
11.61
11.61
11.61
11.61
11.61
11.61
11.61
11.61
11.61
11.61
11.49
11.13
11.13
11.13
11.13
11.13
11.13
11.13
11.13
11.13
11.13
11.13
11.13
%
8.93
8.69
8.81
8.81
8.93
9.05
9.05
8.81
8.93
9.05
8.93
8.93
8.69
8.93
8.93
8.81
8.93
8.81
8.81
8.93
9.05
8.93
8.69
8.69
8.69
8.81
8.81
8.81
8.81
8.93
9.17
9.05
9.05
8.93
8.81
8.81
8.81
8.81
8.57
8.45
8.58
8.74
8.86
8.86
8.86
8.95
8.93
8.93
9.05
24
                                       RCA#2 APPENDIX F

-------
2:26
2:27
2:28
2:29
2:30
2:31
2:32
2:33
2:34
2:35
2:36
2:37
2:38
2:39
2:40
2:41
2:42
2:43
2:44
2:45
2:46
2:47
2:48
2:49
2:50
2:51
2:52
2:53
2:54
2:55
2:56
2:57
2:58
2:59
3:00
3:01
3:02
3:03
3:04
3:05
10.04
9.95
10.67
10.13
11.17
11.74
12.20
11.46
12.30
12.47
11.83
9.83
10.89
10.92
11.42
12.52
12.85
11.30
9.37
9.66
10.08
10.74
10.75
10.78
9.99
9.11
10.17
9.47
10.69
10.16
10.40
10.09








14.52
14.38
15.27
15.80
17.87
20.08
20.44
18.25
18.83
19.36
19.78
21.94
22.66
22.21
16.12
17.31
17.79
16.98
19.36
21.07
20.47
15.38
15.89
15.50
14.95
14.89
13.86
14.24
14.09
13.74
14.88
14.63








11.13
9.78
9.78
9.78
9.78
9.78
9.78
9.78
9.78
9.78
9.78
9.78
9.78
9.78
11.69
12.33
12.33
12.33
12.33
12.33
12.33
12.33
12.33
12.33
12.33
12.33
12.33
11.57
10.81
10.81
10.81
10.81
10.81
10.81
10.81
10.81
10.81
10.81
10.81
10.81
8.93
8.93
8.93
8.81
8.93
9.05
9.05
8.57
8.69
8.57
8.57
8.57
8.81
8.93
8.81
8.81
8.93
8.93
8.81
8.93
8.81
8.93
8.93
8.93
8.69
8.81
8.81
8.81
8.81
8.81
8.69
8.69








Average
Minimum
Maximum
P5B

10.53
8.83
12.85
DR 300-40

  16.92
  13.44
  23.41
F904K

11.15
 9.78
12.33
Moisture

  8.85
  8.45
  9.17
                                                                   82
                                                                   82
                                                                   82
                                                                   82
                                                                   82
                                                                   82
                                                                   82
                                                                   82
                                                                   82
                                                                   82
                                                                   82
                                                                   82
                                                                   82
                                                                   82
                                                                   82
                                                                   82
                                                                   82
                                                                   82
                                                                   82
                                                                   82
                                                                   82
                                                                   82
                                                                   82
                                                                   82
                                                                   82
                                                                   82
                                                                   82
                                                                   82
                                                                   82
                                                                   82
                                                                   82
                                                                   82
Temp

82.12
82.00
84.00
180
                                  RCA#2 APPENDIX F
                                                                                             25

-------
    Run 38
For P5B &
M17 300-40
Results mg/acm
Train A
Train B
Average
36.7

36.7
Single point 24.1
For RSD &
F904K
mg/dscm
51.7

51.7
33.5

Moisture
%
11.4

11.4
10.1
26
                                  RCA#2 APPENDIX F

-------
RCA #2 Testing - Run 39: Mid PM concentration
 11/19/99  ESC P5B  Durag 300-40 Durag F904K  Moisture             Temp.
                                                                degC
                                                                 82
                                                                 82
                                                                 82
                                                                 82
                                                                 82
                                                                 82
                                                                 82
                                                                 82
                                                                 82
                                                                 82
                                                                 82
                                                                 82
                                                                 82
                                                                 82
                                                                 82
                                                                 82
                                                                 82
                                                                 82
                                                                 82
                                                                 82
                                                                 82
                                                                 82
                                                                 82
                                                                 82
                                                                 82
                                                                 82
                                                                 82
                                                                 82
                                                                 82
                                                                 82
                                                                 82
                                                                 82
                                                                 82
                                                                 82
                                                                  82
                                                                  82
                                                                  82
                                                                  82
                                                                  82
                                                                  82
                                                                  82
                                                                  82
                                                                  82
                                                                  82
                                                                  82
                                                                  82
                                                                  82
                                                                  82
                                                                  82
Time
3:36
3:37
3:37
3:38
3:39
3:40
3:41
3:42
3:43
3:44
3:45
3:46
3:47
3:48
3:49
3:50
3:51
3:52
3:53
3:54
3:55
3:56
3:57
3:58
3:59
4:00
4:01
4:02
4:03
4:04
4:05
4:06
4:07
4:08
4:09
4:10
4:11
4:12
4:13
4:14
4:15
4:16
4:17
4:18
4:19
4:20
4:21
4:22
4:23
raw mA
10.59
10.97
10.78
10.62
10.47
10.39
10.62
11.04
11.19
11.11
10.84
12.00
12.06
12.55
11.43
11.82
11.95
11.91
10.37
11.52
11.30
12.22
13.74
13.26
10.80
11.19
10.39
10.25
10.90
11.70
11.25
9.40
9.90
10.65
10.20
10.75
10.09
10.01
10.77
10.19
10.69
11.49
10.17
10.93
11.02
11.03
11.31
11.91
12.31
raw ra mA
15.93
15.23
15.04
14.76
15.50
16.42
14.78
15.95
15.33
15.58
16.41
19.18
22.06
21.88
19.21
19.93
20.62
21.10
25.15
27.16
25.63
17.23
18.67
18.67
17.92
22.45
23.83
18.85
17.48
16.97
17.14
15.24
13.65
14.56
13.97
14.05
14.00
14.33
15.13
14.95
14.54
15.65
16.27
16.95
16.60
16.01
15.73
21.85
22.27
raw mA











11.21
11.21
11.21
11.21
11.21
11.21
11.21
11.21
11.21
11.21
11.21
11.21
11.21
11.51
11.61
11.61
11.61
11.61
11.61
11.61
11.61
11.61
11.61
11.61
11.61
11.61
11.33
11.05
11.05
11.05
11.05
11.05
11.05
11.05
11.05
11.05
11.05
11.05
%
8.93
8.93
8.93
8.93
8.93
8.93
8.93
8.93
8.93
8.81
8.81
9.05
9.05
9.05
8.69
8.81
8.93
8.93
8.93
8.93
8.93
8.81
8.93
8.93
8.93
8.93
8.81
8.69
8.93
8.93
8.93
8.69
8.81
8.93
8.93
8.93
8.93
9.05
9.05
8.93
9.05
8.93
8.93
8.93
8.93
8.93
9.05
9.05
9.05
                                                                                           27
                                  RCA#2 APPENDIX F

-------
4:24
4:25
4:26
4:27
4:28
4:29
4:30
4:31
4:32
4:33
4:34
4:35
4:36
4:37
4:38
4:39
4:40
4:41
4:42
4:43
4:44
4:45
4:46
4:47
4:48
4:49
4:50
4:51
4:52
4:53
4:54
4:55
4:56
4:57
4:58
4:59
5:00
5:01
5:02
5:03
5:04
5:05
5:06
5:07
5:08
5:09
12.50
11.18
12.64
12.30
10.42
9.89
11.12
10.50
11.93
12.45
11.97
9.59
9.71
9.68
10.09
10.66
11.20
11.06
9.64
10.01
9.48
9.97
10.96
11.40
9.97
10.51
10.21
11.23
10.95
11.72
11.48
10.48
11.04
10.94
12.15
12.15
13.05
11.94
12.19
12.52
10.48





22.21
17.93
19.69
19.42
19.45
25.18
24.13
21.19
17.44
17.66
17.55
18.64
20.98
21.28
16.80
17.50
17.59
16.15
14.34
14.97
14.51
15.07
15.79
15.12
15.98
16.25
16.53
15.84
15.69
16.21
16.14
15.58
16.10
17.02






21.82





11.05
11.11
11.29
11.29
11.29
11.29
11.29
11.29
11.29
11.29
11.29
11.29
11.29
11.29
11.29
11.69
11.69
11.69
11.69
11.69
11.69
11.69
11.69
11.69
11.69
11.69
11.69
11.69
11.09
10.89
10.89
10.89
10.89
10.89
10.89
10.89
10.89
10.89
10.89
10.89
10.89
11.53
12.16
12.16
12.16
12.16
9.05
8.69
8.93
8.93
8.93
8.93
8.93
9.05
8.93
8.93
8.93
8.93
8.93
8.93
8.81
8.93
9.05
8.93
8.93
9.05
9.05
8.81
8.81
8.93
8.81
9.05
9.05
9.05
9.05
9.05
9.17
9.17
9.17
9.17
9.17
9.17
9.05
8.69
8.93
8.93
9.05





      Average
      Minimum
      Maximum
P5B

11.08
9.40
13.74
DR 300-40

  17.76
  13.65
  27.16
F904K

11.34
10.89
12.16
Moisture

  8.95
  8.69
  9.17
                                                                        82
                                                                        82
                                                                        82
                                                                        82
                                                                        82
                                                                        82
                                                                        82
                                                                        82
                                                                        82
                                                                        82
                                                                        82
                                                                        82
                                                                        82
                                                                        82
                                                                        82
                                                                        82
                                                                        82
                                                                        82
                                                                        82
                                                                        82
                                                                        82
                                                                        82
                                                                        82
                                                                        82
                                                                        82
                                                                        82
                                                                        82
                                                                        82
                                                                        82
                                                                        82
                                                                        82
                                                                        82
                                                                        82
                                                                        82
                                                                        82
                                                                        82
                                                                        82
                                                                        82
                                                                        82
                                                                        82
                                                                        82
Temp

82.00
82.00
82.00
180
28
                                        RCA#2 APPENDIX F

-------
Run 39
For P5B &
M17 300-40
Results mg/acm
Train A
Train B
Average
35.6

35.6
Single point 24.5
For BSD &
F904K
mg/dscm
49.5

49.5
34.1

Moisture
%
10.4

10.4
10.3
                              RCA#2 APPENDIX F
                                                                                29

-------
      RCA #2 Testing - Run 40: Low PM concentration
                                                                    Temp.
                                                                    deg C
                                                                      84
                                                                      84
                                                                      84
                                                                      84
                                                                      84
                                                                      84
                                                                      83
                                                                      82
                                                                      82
                                                                      82
                                                                      82
                                                                      82
                                                                      82
                                                                      82
                                                                      82
                                                                      83
                                                                      84
                                                                      84
                                                                      84
                                                                      84
                                                                      84
                                                                      84
                                                                      82
                                                                      82
                                                                      82
                                                                      82
                                                                      82
                                                                      82
                                                                      83
                                                                      84
                                                                      84
                                                                      84
                                                                      84
                                                                      84
                                                                      84
                                                                      82
                                                                      82
                                                                      82
                                                                      82
                                                                      82
                                                                      82
                                                                      82
                                                                      82
                                                                      82
                                                                      83
                                                                      84
                                                                      84
                                                                      84
                                                                      84
11/20/99
Time
9:00
9:01
9:02
9:03
9:04
9:05
9:06
9:07
9:08
9:09
9:10
9:11
9:12
9:13
9:14
9:15
9:16
. 9:17
9:18
9:19
9:20
9:21
9:22
9:23
9:24
9:25
9:26
9:27
9:28
9:29
9:30
9:31
9:32
9:33
9:34
9:35
9:36
9:37
9:38
9:39
9:40
9:41
9:42
9:43
9:44
9:45
9:46
9:47
9:48
ESC P5B
raw mA
6.49
6.75
6.82
6.59
6.49
6.30
6.53
6.70
6.33
6.53
6.79
6.81
7.54
7.77
7.93
6.40
6.42
6.66
6.69
6.93
6.84
6.84
6.18
6.21
6.16
6.22
6.10
6.28
6.16
6.28
6.38
6.32
6.23
6.45
6.29
6.45
6.43
6.46
6.32
6.63
6.54
6.54
6.48
6.82
6.49
6.50
6.62
6.76
6.71
Durag 300-40
raw ra mA
8.17
8.02
9.34
8.08
7.73
7.22
7.76
8.05
8.78
10.71
11.46
9.92
8.22
8.82
9.15
9.01
10.42
10.49
8.68
8.55
8.35
8.08
7.09
7.26
7.41
7.33
7.29
7.21
7.17
7.12
7.06
7.39
7.30
7.00
7.17
7.22
7.49
7.55
7.68
7.91
7.81
7.63
7.48
7.39
8.03
8.23
8.08
7.91
8.07
Durag F904K
raw mA











6.02
6.02
6.02
6.02
6.02
6.02
6.02
6.02
6.02
6.02
6.02
6.02
6.02
6.65
6.65
6.65
6.65
6.65
6.65
6.65
6.65
6.65
6.65
6.65
6.65
6.65
6.35
6.25
6.25
6.25
6.25
6.25
6.25
6.25
6.25
6.25
6.25
6.25
Moistur
%
10.07
10.20
10.32
9.71
9.10
8.01
7.99
7.97
8.09
8.09
8.21
8.21
8.33
8.69
8.81
8.96
8.98
8.86
8.62
8.50
8.25
8.00
7.85
7.72
7.48
7.36
7.24
7.24
7.50
7.53
7.65
8.13
8.38
8.62
9.10
9.41
9.29
9.05
9.29
9.17
9.05
8.93
8.93
8.93
9.31
9.71
9.83
9.71
9.71
30
                                      RCAS2 APPENDIX F

-------
9:49
9:50
9:51
9:52
9:53
9:54
9:55
9:56
9:57
9:58
9:59
10:00
10:01
10:02
10:03
10:04
10:05
10:06
10:07
10:08
10:09
10:10
10:11
10:12
10:13
10:14
10:15
10:16
10:17
10:18
10:19
10:20
10:21
10:22
10:23
10:24
10:25
10:26
10:27
10:28
10:29
6.79
6.79
6.77
7.45
7.31
7.23
7.11
6.93
7.28
6.66
6.70
6.93
7.18
7.82
8.29
8.33
6.76
7.41
7.44
7.61
8.81
9.67
11.22
11.30
12.85
13.84
13.46
13.30
13.77
13.51
10.82
11.55









8.59
8.33
8.39
9.19
9.45
9.52
8.99
8.96
9.22
9.77
11.79
12.06
11.77
9.17
9.55
10.19
10.68
12.73
14.83
12.97
12.93
14.73
16.80
18.55
22.75
25.69
23.53
25.36
27.52
29.20
35.86
40.03









6.25
6.25
6.25
6.25
6.25
6.25
6.25
6.25
6.25
6.25
6.25
6.25
6.25
6.25
6.15
5.85
5.85
5.85
5.85
5.85
5.85
5.85
5.85
5.85
5.85
5.85
5.85
6.15
7.05
7.05
7.05
7.05
7.05
7.05
7.05
7.05
7.05
7.05
7.05
7.05
7.05
9.71
9.71
9.71
9.83
9.95
9.95
9.59
9.71
9.70
9.54
9.55
9.59
9.83
10.07
10.20
10.07
10.20
10.44
10.56
10.56
10.80
11.05
11.05
11.17
11.29
11.29
10.92
10.80
10.56
10.44
10.32
10.20









Average
Minimum
Maximum
P5B

7.54
6.10
13.84
DR 300-40

  11.07
  7.00
  40.03
F904K

 6.35
 5.85
 7.05
Moisture

  9.29
  7.24
 11.29
                                                                   84
                                                                   84
                                                                   84
                                                                   84
                                                                   84
                                                                   84
                                                                   84
                                                                   84
                                                                   84
                                                                   82
                                                                   83
                                                                   84
                                                                   84
                                                                   84
                                                                   84
                                                                   84
                                                                   84
                                                                   84
                                                                   84
                                                                   84
                                                                   84
                                                                   84
                                                                   84
                                                                   84
                                                                   84
                                                                   84
                                                                   84
                                                                   84
                                                                   84
                                                                   84
                                                                   84
                                                                   84
Temp

83.35
82.00
84.00
                                                                             182
                                   RCA#2 APPENDIX F
                                                                                             31

-------
    Run 40
For P5B &
M17 300-40
Results mg/acm
Train A
Average
12.2
12.2
Single point 10.2
For BSD &
F904K
mg/dscm
17.5
17.5
14.7
Moisture
%
12.4
12.4
12.4
32
                                   RCA#2 APPENDIX F

-------
RCA #2 Testing - Run 41: Low PM concentration
 11/20/99  ESC P5B  Durag 300-40 Durag F904K  Moisture             Temp.
                                                               degC
                                                                 84
                                                                 84
                                                                 84
                                                                 84
                                                                 84
                                                                 84
                                                                 84
                                                                 84
                                                                 84
                                                                 84
                                                                 84
                                                                 84
                                                                 84
                                                                 84
                                                                 84
                                                                 84
                                                                 84
                                                                 84
                                                                 84
                                                                 84
                                                                 84
                                                                 84
                                                                 84
                                                                 84
                                                                 84
                                                                 84
                                                                 84
                                                                 84
                                                                 84
                                                                 84
                                                                 84
                                                                 84
                                                                 84
                                                                 84
                                                                 84
                                                                 84
                                                                 84
                                                                 84
                                                                 84
                                                                 84
                                                                 84
                                                                 84
                                                                 84
                                                                 84
                                                                 84
                                                                 84
                                                                 84
                                                                 83
                                                                 82
Time
11:12
11:13
11:14
11:15
11:16
11:17
11:18
11:19
11:20
11:21
11:22
11:23
11:24
11:25
11:26
11:27
11:28
11:29
11:30
11:31
11:32
11:33
11:34
11:35
11:36
11:37
11:38
11:39
11:40
11:41
11:42
11:43
11:44
11:45
11:46
11:47
11:48
11:49
11:50
11:51
11:52
11:53
11:54
11:55
11:56
11:57
11:58
11:59
12:00
raw mA
6.58
7.00
6.77
6.77
7.31
7.56
7.25
6.54
6.86
6.88
7.08
7.17
7.12
7.59
7.47
7.98
7.42
7.72
7.86
7.74
7.78
8.06
7.70
8.72
8.48
8.34
8.05
8.23
8.43
7.40
7.27
7.30
7.27
9.15
9.32
8.92
6.84
7.12
7.42
7.55
8.16
8.26
7.84
7.18
6.71
6.89
7.05
6.85
6.80
raw ra mA
10.13
11.52
12.17
9.24
9.46
9.77
9.93
8.28
8.74
8.45
9.13
9.45
9.74
9.46
9.57
10.11
10.14
9.79
9.63
10.49
10.42
10.59
10.32
12.83
12.89
12.39
11.85
11.85
11.86
12.74
16.02
15.53
13.26
11.05
11.58
11.46
11.87
13.89
14.13
11.34
12.15
11.45
10.90
8.83
8.73
8.68
8.49
8.78
9.02
raw mA











7.30
7.30
7.30
7.30
7.30
7.30
7.30
7.30
7.30
7.30
7.30
7.30
7.30
7.60
7.70
7.70
7.70
7.70
7.70
7.70
7.70
7.70
7.70
7.70
7.70
7.70
7.94
8.18
8.18
8.18
8.18
8.18
8.18
8.18
8.17
8.18
8.18
8.18
%
8.62
8.62
8.50
8.25
8.50
8.62
8.62
8.62
8.62
8.62
8.74
8.74
8.74
8.62
8.38
8.62
8.74
8.62
8.50
8.50
8.50
8.50
8.50
8.74
8.74
8.74
8.50
8.62
8.62
8.62
8.62
8.62
8.62
8.62
8.62
8.86
8.86
8.98
8.98
8.74
8.98
8.86
8.62
8.62
8.62
8.74
8.74
8.71
9.17
                                                                                          33
                                 RCA#2 APPENDIX F

-------
12:01
12:02
12:03
12:04
12:05
12:06
12:07
12:08
12:09
12:10
12:11
12:12
12:13
12:14
12:15
12:16
12:17
12:18
12:19
12:20
12:21
12:22
12:23
12:24
12:25
12:26
12:27
12:28
12:29
12:30
12:31
12:32
12:33
12:34
12:35
12:36
12:37
12:38
12:39
12:40
12:41
7.10
7.18
7.38
8.13
8.48
8.32
7.58
8.05
8.43
7.88
8.28
9.30
9.77
12.70
14.78
15.66
11.23
11.68
11.77
11.38
12.52
12.88
13.60
13.14
14.14
14.37
12.99
12.95
13.46
12.77
10.43
10.41









8.98
9.39
9.73
11.58
12.52
12.02
11.32
11.95
12.75
14.40
20.89
24.52
25.39
18.85
21.49
23.41
26.11
29.77
31.51
27.40
24.04
24.25
24.61
23.20
25.75
26.71
23.83
24.79
24.58
24.37
32.56
34.12









8.18
7.80
6.65
6.65
6.65
6.65
6.65
6.65
6.65
6.65
6.65
6.65
6.65
6.65
6.65
7.05
7.05
7.05
7.05
7.05
7.05
7.05
7.05
7.05
7.05
7.05
7.05
7.05
10.33
10.33
10.33
10.33
10.33
10.33
10.33
10.33
10.33
10.33
10.33
10.33
10.33
9.05
9.05
8.93
9.05
9.10
9.22
9.10
9.83
9.82
9.90
9.66
9.90
10.02
10.26
10.26
10.26
10.41
10.44
10.44
10.44
10.32
10.04
9.78
9.90
9.90
9.78
9.54
9.66
9.66
9.66
9.54
9.66









      Average
      Minimum
      Maximum
P5B

8.87
6.54
15.66
DR 300-40

  14.90
  8.28
  34.12
F904K

 7.86
 6.65
 10.33
Moisture

  9.10
  8.25
 10.44
                                                                         82
                                                                         82
                                                                         82
                                                                         82
                                                                         84
                                                                         84
                                                                         84
                                                                         84
                                                                         84
                                                                         82
                                                                         82
                                                                         82
                                                                         82
                                                                         82
                                                                         82
                                                                         82
                                                                         83
                                                                         84
                                                                         84
                                                                         84
                                                                         84
                                                                         83
                                                                         82
                                                                         82
                                                                         82
                                                                         82
                                                                         82
                                                                         82
                                                                         82
                                                                         82
                                                                         82
                                                                         82
Temp

83.42
82.00
84.00
182
34
                                         RCA#2 APPENDIX F

-------
Run 41
For P5B &
M17 300-40
Results mg/acm
Train A
Average
24.1
24.1
Single poin 13.8
For BSD &
F904K
mg/dscm
34.7
34.7
20
Moisture
%
12.4
12.4
12.4
                             RCA#2 APPENDIX F
                                                                                35

-------
      RCA #2 Testing - Run 42: High PM concentration
       11/20/99  ESC P5B Durag 300-40 Durag F904K  Moisture             Temp.
                                                                      degC
                                                                       84
                                                                       84
                                                                       84
                                                                       85
                                                                       86
                                                                       86
                                                                       86
                                                                       86
                                                                       86
                                                                       86
                                                                       86
                                                                       86
                                                                       85
                                                                       84
                                                                       84
                                                                       84
                                                                       84
                                                                       84
                                                                       84
                                                                       84
                                                                       84
                                                                       84
                                                                       84
                                                                       84
                                                                       84
                                                                       84
                                                                       84
                                                                       84
                                                                       84
                                                                       84
                                                                       84
                                                                       84
                                                                       84
                                                                       84
                                                                       84
                                                                       84
                                                                       84
                                                                       84
                                                                       84
                                                                       84
                                                                       84
                                                                       84
                                                                       84
                                                                       84
                                                                       84
                                                                       84
                                                                       84
                                                                       84
                                                                       84
Time
13:50
13:51
13:52
13:53
13:54
13:55
13:56
13:57
13:58
13:59
14:00
14:01
14:02
14:03
14:04
14:05
14:06
14:07
14:08
14:09
14:10
14:11
14:12
14:13
14:14
14:15
14:16
14:17
14:18
14:19
14:20
14:21
14:22
14:23
14:24
14:25
14:26
14:27
14:28
14:29
14:30
14:31
14:32
14:33
14:34
14:35
14:36
14:37
14:38
rawmA
14.93
15.56
12.29
14.61
15.48
16.87
19.73
19.96
16.55
17.04
17.37
15.88
15.98
16.69
18.27
18.22
19.67
19.39
18.54
15.40
16.70
16.86
12.36
10.48
10.61
10.52
12.42
12.54
10.16
8.48
8.69
8.79
8.87
9.43
9.52
8.87
8.67
8.80
9.12
7.96
8.70
9.61
8.29
8.16
8.97
9.17
11.30
12.34
11.26
raw ra mA
27.13
31.60
39.55
44.71
45.58
32.05
36.37
37.84
41.08
143.41
56.29
81.67
36.61
37.84
36.70
36.55
39.07
37.48
34.09
32.23
33.70
32.65
35.65
37.03
33.13
21.52
20.74
20.38
18.30
19.60
21.04
21.10
16.00
16.55
17.37
14.33
13.12
13.05
12.96
12.24
13.11
15.13
16.72
21.40
22.93
21.34
16.68
18.09
17.57
raw mA












12.01
12.01
12.01
12.01
12.01
12.01
12.01
12.01
12.01
12.01
12.01
12.01
12.01
13.28
13.28
13.28
13.28
13.28
13.28
13.28
13.28
13.28
13.28
13.28
13.28
13.28
10.53
9.61
9.61
9.61
9.61
9.61
9.61
9.61
9.61
9.61
9.61
%
8.50
8.74
8.74
8.88
.9.03
9.03
9.15
9.28
9.28
9.40
9.40
9.15
9.24
9.22
9.10
8.98
9.10
8.98
8.62
8.62
8.62
8.74
8.62
8.13
7.89
7.65
7.40
7.53
7.53
7.77
8.13
8.01
8.38
8.38
8.38
8.25
8.25
8.13
8.13
7.77
8.01
8.13
8.25
8.38
8.50
8.50
8.25
8.25
8.38
36
                                       RCA#2 APPENDIX F

-------
14:39
14:40
14:41
14:42
14:43
14:44
14:45
14:46
14:47
14:48
14:49
14:50
14:51
14:52
14:53
14:54
14:55
14:56
14:57
14:58
14:58
14:59
15:00
15:01
15:01
15:02
15:03
15:04
15:05
15:06
15:07
15:08
15:09
15:10
15:11
15:12
15:13
15:14
15:15
15:16
15:17
15:18
15:19
15:20
15:21
15:22
15:23
15:24
15:25
15:26
8.92
9.27
9.74
9.93
11.78
11.80
12.11
12.12
11.99
12.82
10.65
11.70
12.36
10.34
9.82
9.92
10.73
12.38
13.93
13.98
12.84
12.44
10.81
10.84
10.79
11.50
13.38
13.42
13.44
13.68
16.00
16.18
15.14
16.47
17.17
16.12














17.68
21.61
22.30
19.87
21.88
21.58
20.95
20.86
22.63
22.57
19.93
21.82
23.62
23.50
29.71
30.55
31.15
18.79
22.18
22.06
22.09
22.75
27.04
28.24
28.87
23.98
25.12
23.89
24.10
24.49
29.44
31.90
30.82
32.98
35.59
38.08














9.61
9.61
9.74
9.78
9.78
9.78
9.78
9.78
9.78
9.78
9.78
9.78
9.78
9.78
9.78
9.81
9.85
9.85
9.85
9.85
9.85
9.85
9.85
9.85
9.85
9.85
9.85
9.85
9.85
9.85
9.97
10.09
10.09
10.09
10.09
10.09
10.09
10.09
10.09
10.09
10.09
10.09
10.09
10.85
13.13
13.13
13.13
13.13
13.13
13.13
8.25
8.13
8.13
8.01
8.25
8.38
8.13
8.25
8.50
8.74
8.38
8.50
8.38
8.38
8.25
8.25
8.13
8.01
8.25
8.25
8.25
8.25
8.25
8.38
8.38
8.13
8.38
8.50
8.25
8.50
8.86
8.98
8.86
9.22
9.35
9.35














                               84
                               84
                               84
                               84
                               84
                               84
                               84
                               84
                               84
                               84
                               84
                               84
                               84
                               84
                               84
                               84
                               84
                               84
                               84
                               84
                               84
                               84
                               84
                               84
                               84
                               84
                               84
                               84
                               84
                               84
                               84
                               84
                               84
                               84
                               84
                               84
                                                        37
RCA#2 APPENDIX F

-------

Average
Minimum
Maximum
P5B
12.74
7.96
19.96
DR 300-40
28.30
12.24
143.41
F904K
10.92
9.61
13.28
Moisture
8.47
7.40
9.40
     Run 42
                                                                      Temp
                                                                      84.21
                                                                      84.00
                                                                      86.00
184
For P5B &
M17 300-40
Results mg/acm
Train A
Average
38.3
38.3
Single point 22.8
For BSD &
F904K
mg/dscm
55.4
55.4
32.8
                                                           Moisture
                                                              %
                                                             12.4

                                                             12.4

                                                             11.2
38
                                        RCA#2 APPENDIX F

-------
                                RCA #2 Appendix G
    Statistical Analysis Data and Graphs from Initial
                         Correlation and RCA Data
MR]-OPPT\R4703-02-07 Appendices Covers WPD

-------
                                                        ESC P5B - Linear
w

H
Q
          O
          IB
          •
             60
             50
             40
             30
20
             10
                  VL = Variable Load
                  LL = Low Load
                        y = 1 .89x - 7.50
                                                                                 LL •
                                                                             VL
                                                                LL
             -10
                                                           10
                                                          mA
                                                            12
14
                                                                                              *   Init. Corr.
                                                                                              A   RCA#1
                                                                                              «•   3 MET coal runs
                                                                                              •   RCA#2
                                                                                              	Correlation Line
                  	 25% Tl
                  	+ 25% Tl

-------
Table G-l. ESC Light Scatter - Linear
Run
13
14
15
16
17
18
19
20
21
22
23
24
1
2
, 3
4
5
6
7
8
9
10
11
12
10
11
12
31
32
33
34
35
36
37
38
39
40
41
42
x(mA)
9.60
10.01
10.54
5.87
5.78
6.00
12.00
9.45
8.97
13.16
9.57
14.50
14.66
6.38
6.41
6.40
8.51
8.35
7.70
10.34
11.23
11.92
9.07
10.17
11.40
11.76
13.88
11.69
10.06
9.60
9.42
7.95
11.00
13.44
10.53
11.08
7.54
8.87
12.74
y (mg/acm)
11.61
13.92
14.47
3.03
2.68
3.20
16.33
10.52
9.42
15.39
8.76
18.66
28.09
1.90
2.55
2.59
9.77
8.29
11.30
22.12
24.05
26.62
12.97
19.10
26.13
27.76
32.28
25.40
19.10-
18.45
10.30
13.60
26.60
57.60
36.70
35.60
12.20
24.10
38.30
ylin
10.62
11.40 i
12.40
3.58 ;
3.41
3.83
15.16
10.34
9.43
17.35
10.57
19.88
RCA #1 data











Three MET coal runs during initial correlation tests.


RCA #2 data











      RCA#2 APPENDIX G

-------
o
                                                   Durag DR 300-40 - Linear
             60
                 VL = Variable Load
                 LL = Low Load
                          LL
                       y = 0.71 x- 0.82
                                                       LL
                                        VL»
             30
          I
          "§>
          £
VL
             10
                                       12
     16
20
24
28
            -10
                                          *   Init. Corr.
                                          A   RCA#1
                                          *   3 MET coal runs
                                          •   RCA#2
                                        	Correlation Line
                                        	25% Tl
                                        	+ 25% Tl
                                                  Range adjusted mA
  co

-------
Table G-3. Durag Light Scatter - Linear
Run
13
14
15
16
17
18
19
20
21
22
23
24
1
2
3
4
5
6
7
8
9
10
11
12
10
11
12
31
32
33
34
35
36 '
37
38
39
40
41
42
x (mA) y (mg/acm)
15.45
17.22
19.36
6.42
6.44
7.28
20.93
15.80
14.32
24.54
15.68
30.88
28.77
6.11
6.59
6.75
11.72
11.92
10.80
16.22
18.60
21.53
12.62
14.59
20.06 =.
21.82-'"
27.83
22.41 ^
18.64-"'
17.77
17.32
13.31
22.72
23.69
16.92
17.76
11.07
14.90
28.30
11.61
13.92
14.47
3.03
2.68
3.20
16.33
10-.52
9.42
15.39
8.76
18.66
28.09
1.90
2.55
2.59
9.77
8.29
11.30
22.12
24.05
26.62
12.97
19.10
26.13
27.76
32.28
25.40
19.10
18.45;
10.30
13.50
26.60
57.60
36.70
35.50
12.20
24.10
38.30
ylin
10.14 i
11.39
12.91
3.73
3.75 ;
4.34 !
14.02
10.38
9.33
16.58
10.30 ;
21.08
RCA #1 data











Three MET coal runs during initial correlation tests.


RCA #2 data











      RCA#2 APPENDIX G

-------
Durag F904K - Linear



w
8
>
5t
NJ
1
tn
R





»7l/
fin
yn
fin -

cri _
o
U) ._
u)
on -

on -
m -
n -
i
-m -
VL = Variable Load
LL = Low Load
LL
y = 3.37x- 12.38

VI •
VL • LL
• + ' ' '
t
* A ^--
**•
Emission Limit = 25,5 mg/dscm A ^^"^ ^ — ^
^--""T ^--^^1--"
^-^~ j^*^^ -'""'
*^
6 8 10 12 14 1




* Init. Corr.
A RCA#1
* 3 MET coal runs
• Dr'AWO
nL»r\fft
	 Correlation Line
	 	 25% Tl
	 + 25% Tl



3
   mA

-------
Table G-2. Durag Beta Gauge - Linear
Run
13
14
15
16
17
18
19
20
21
22
23
24
1
2
3
4
5
e
7
8
9
10
11
12
10
11
12
31
32
33
34
35
36
37
38
39
40
41
42
x (mA) y (mg/dscm)
8.58
9.24
9.98
5.04
5.09
5.21
10.48
8.07
8.05
10.95
8.08
12.57
14.20
5.04
5.07
4.99
7.30
6.99
6.88
9.71
10.71
11.65
7.57
8.42
11.74 '
11.71 ..
14.49
ProS-i £>»-<
''
/)
>'
7.14
10.28
14.80
11.15
11.34
6.35
7.86
10.92
17.20
21.10
21.75
4.60
4.00
4.80
24.40
16.10
14.30
23.25
13.05
28.35
43.05
2.90
3.95
4.00
14.80
12.65
17.40
33.65
36.60
41.00
19.45
28.65
39.50
41.80
49.55
)'K
-------
                                  TECHNICAL REPORT DATA
                              (Please read Instructions on reverse before completing)
1. RfiPORT NO.
  EPA-454/R-00-040d
                                                                3. RECIPIENT'S ACCESSION NO.
4. TITLE AND SUBTITLE
EVALUATION OF PARTICIPATE MATTER CONTINUOUS EMISSION
MONITORING SYSTEMS
Volume 4
5. REPORT DATE September 2000
                                                                6. PERFORMING ORGANIZATION CODE
7. AUTHOR(S) Dan Bivins
Emission Monitoring and Analysis Division
                                                                8. PERFORMING ORGANIZATION REPORT NO.
). PERFORMING ORGANIZATION NAME AND ADDRESS

  U.S. Environmental Protection Agency
  Office of Air Quality Planning and Standards
  Research Triangle Park, NC 27711
                                                                10. PROGRAM ELEMENT NO.
11. CONTRACT/GRANT NO.
68-D-98-027
2. SPONSORING AGENCY NAME AND ADDRESS
  Director
  Office of Air Quality Planning and Standards
  Office of Ak and Radiation
  U.S. Environmental Protection Agency
  Research Triangle Park, NC 27711	
13. TYPE OF REPORT AND PERIOD COVERED
Final
14. SPONSORING AGENCY CODE
EPA/200/04
 i. SUPPLEMENTARY NOTES
 i. ABSTRACT
 his final report describes an extended field demonstration of three particulate matter (PM) continuous
 mission monitoring systems (CEMS) at a coal-fired boiler equipped with a lime slurry scrubber and
 aghouse for air pollution control.  The primary objectives of the field study were to: (1) demonstrate whether
 le PM CEMS could provide reliable and accurate data over an extended period, (2) evaluate the PM CEMS
 >r durability, data availability, and setup/maintenance requirements, and (3) determine whether the PM
 EMS satisfy all the requirements  of draft PS-11 and the quality assurance (QA) criteria specified in draft
 rocedure 2, or determine if changes are needed in the requirements of PS-11 and/or Procedure 2.  This
 port presents the results of the study involving two different PM CEMS technologies (light scatter and beta
 mge) at the coal-fired boiler.  The report consists of five separate volumes.
KEY WORDS AND DOCUMENT ANALYSIS
DESCRIPTORS
•11
thod 17
icedure 2
•isture CEMS
•nonstranon
nculate Matter
CEMS
DISTRIBUTION STATEMENT
Release Unlimited
b. IDENTIFIERS/OPEN ENDED TERMS
Air Pollution control
19. SECURITY CLASS (Report]
Unclassified
20. SECURITY CLASS (Page)
Unclassified
c. COSATI Field/Group

21. NO. OF PAGES
280
22. PRICE
  form 2220-1 (Rev. 4-77)   PREVIOUS EDITION IS OBSOLETE

-------