EPA-450/2-78-001
January 1978
AIR QUALITY DATA
FOR NON-CRITERIA POLLUTANTS
1971 THROUGH 1975
U.S. ENVIRONMENTAL PROTECTION AGENCY
Office of Air and Waste Management
Office of Air Quality Planning and Standards
Research Triangle Park, North Carolina 27711
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EPA-450/2-78-001
AIR QUALITY DATA
FOR NON-CRITERIA POLLUTANTS -
1971 THROUGH 1975
Monitoring and Data Analysis Division
U.S. ENVIRONMENTAL PROTECTION AGENCY
Office of Air and Waste Management
Office of Air Quality Planning and Standards
Research Triangle Park, North Carolina 27711
January 1978
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This report has been reviewed by the Monitoring and Data Analysis Division, Off ice of Air Quality
Planning and Standards, Office of Air and Waste Management, Environmental Protection
Agency, and approved for publication. Mention of company or product names does not
constitute endorsement by EPA. Copies are available free of charge to Federal employees,
current contractors and grantees, and non-profit organizations - as supplies permit - from the
Library Services Office (MD-35), U.S. Environmental Protection Agency, Research Triangle
Park, North Carolina 27711; or may be obtained, for a nominal cost, from the National Technical
Information Service, 5285 Port Royal Road, Springfield, Virginia 22161.
Publication No. EPA-450/2-78-001
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CONTENTS
Page
INTRODUCTION M
SAMPLE COLLECTION AND ANALYSIS |_1
DESCRIPTION OF DATA TABLES -M
DATA TABLES 1
Benzene - Soluble Organic Fraction 1
Aluminum 17
Antimony 12
Arsenic 19
Beryllium 24
Bismuth 34
Cadmium 35
Calcium 5g
Chromium 60
Cobalt 78
Copper 96
lron 118
Lead 143
Manganese 176
Molybdenum
Nickel
Mercury 2U
Tin .'. 215
Titanium
Vanadium 244
Zinc .'.'.'.'.'.'.'.'.'.'.'.'.'.'.'.'.'.'.'.'.'.'.'.'.'.'.'.'.'.'.'.'.'.'.'.'.' 261
Strontium 266
Fluoride Ion 267
Chloride Ion 270
Ammonium Ion 272
Nitrate Ion 280
Phosphate Ion 3og
Sulfate Ion 310
BIBLIOGRAPHIC DATA SHEET 345
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AIR QUALITY DATA
FOR NON-CRITERIA POLLUTANTS -
1971 THROUGH 1975
INTRODUCTION
The Storage and Retrieval of Aerometric Data (SAROAD) System is the established data bank
within the U.S. Environmental Protection Agency for the storage and retrieval of ambient air quality
data resulting from air monitoring operations of State, local, and Federal networks. The SAROAD
System is a part of the EPA Aerometric and Emissions Reporting System (AEROS), which is managed
by the National Air Data Branch (NADB), Monitoring and Data Analysis Division, Office of AirQuality
Planning and Standards.
Major portions of the data stored in SAROAD are for the criteria pollutants (particulate matter,
sulfur dioxide, carbon monoxide, nitrogen dioxide, photochemical oxidants, and hydrocarbons)
and are received from State and local agencies as required by regulations for State Implementation
Plans (SIPS).1 These data have been routinely published for 1968 to 1976 by EPA in "Air Quality Data
19XX Annual Statistics."
This publication is the second in a series concerning pollutants that do not have National Ambient Air
Quality Standards but that have been reported to SAROAD. The first publication contained data for
1957-70. This second publication, like the first, is limited to pollutants that are collected on a high-
volume sampler filter as particulate matter and chemically analyzed for the specific elements or ions.
These specific pollutants are listed in Table 1 with the specific analysis methods and minimum
detectable values.
Rather than complete summary statistics or raw data, this publication provides an inventory of
these pollutants for 1971-1975. Additional reports for these pollutants such as raw data, summary
statistics, or site information are available upon request from NADB or the appropriate EPA Regional
Office. The SAROAD contact offices at each Regional Office are shown in Table 2. Requests may be
subject to charges to recover direct retrieval costs incurred by the Government.
SAMPLE COLLECTION AND ANALYSIS
As previously discussed, the data for the pollutants in Table 1 were produced by analysis of
particulate matter that was collected on high-volume filters. Most State and local agencies can
analyze this particulate matter for trace pollutants. A review of this publication indicates that several
reported the data to SAROAD for 1971-1975. The majority of the data in this publication was collected
and reported by the National Air Sampling Network. These data are reported with an agency code
of 'A'.
Operational since 1957, the National Air Sampling Network (NASN) has varied in size from 200-
300 urban and 20-30 non-urban sites located across the nation. Operation of the NASN sites has
been maintained through assistance of local or State agencies as well as individuals such as park
rangers, firemen, and policemen. The NASN sites operated on a biweekly modified random sampling
schedule from midnight to midnight to provide 26 samples per year. Beginning in January, 1972, the
sampling schedule was changed to a sample every 12th day which insured equal representation for
everyday of the week and produced 30 or 31 samples per year.
'Federal Register, Vol. 38, No. 149, Friday, August 3, 1973, pp. 20834 and 20835.
1-1
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Table 1. POLLUTANT AND MINIMUM DETECTABLE CONCENTRATION
Pollutant
Benzene-soluble
organic fraction
Aluminum
Antimony
Arsenic
Beryllium
Bismuth
Cadmium
Calcium
Chromium
Cobalt
Copper
Iron
Lead
Manganese
Molybdenum
Nickel
Mercury
Analysis method
Benzene Extraction - Soxhlet
Atomic absorption
Atomic absorption
Atomic absorption
NASA arsine-colorimetric
X-ray fluorescence
Atomic absorption
Emission spectra - low-temperature ash
Atomic absorption
Emission spectra - muffle furnace
Atomic absorption
Emission spectra - low-temperature ash
Atomic absorption
Atomic absorption
Emission spectra - low-temperture ash
Emission spectra - muffle furnace
Atomic absorption
Emission spectra - low-temperature ash
Emission spectra - muffle furnace
Atomic absorption
Emission spectra - low temperature ash
Emission spectra - muffle furnace
Atomic absorption
Emission spectra - low-temperature ash
Emission spectra - muffle furnace
Atomic absorption
Emission spectra - low-temperature ash
X-ray fluorescence
Atomic absorption
Emission spectra - low-temperature ash
Atomic absorption
Atomic absorption
Emission spectra - low-temperature ash
Atomic absorption
Urban
minimum
detectable,
jug/m3
0.2
0.01
0.0002
0.02
0.02
0.05
0.0002s
0.23
0.001
0.002
0.0002
0.002
0.0002
0.002
0.006
0.004
0.004
0.004
0.01
0.001
0.01
0.1
0.01
0.1
0.01
0.002
0.01
0.05
0.001
0.01
0.002
0.004
0.005
0.0001
Non-urban
minimum
detectable,
jug/m3
0.1
0.01
0.0002
0.02
0.02
0.05
0.00023
0.0?a
0.0004
0.0006
0.0002
0.0006
0.0002
0.002
0.002
0.001
0.001
0.001
0.003
0.001
0.003
0.03
0.01
0.03
0.004
0.002
0.004
0.05
0.001
0.004
0.0008
0.004
0.002
0.0001
I-2
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Table 1 (cont'd). POLLUTANT AND MINIMUM DETECTABLE CONCENTRATION
Pollutant
Tin
Titanium
Vanadium
Zinc
Strontium
Fluoride ion
Chloride ion
Ammonium ion
Nitrate ion
Phosphate ion
Sulfate ion
Analysis method
Atomic absorption
Emission spectra - low-temperature ash
Atomic absorption
Emission spectra - low-temperature ash
Atomic absorption
Emission spectra - low-temperature ash
Atomic absorption
Emission spectra - low-temperature ash
Willard - winter - specific ion
Thiocyanate
Sodium phenolate
2-4 Xylenol
Reduction diazo coupling
Specific ion electrode
Ultraviolet specrophotometric
Molybdate - stannous chloride
Colorimetric
Turbidimetric
Urban
minimum
detectable,
/ig/m3
0.001
0.001
0.01
0.01
0.01
0.003
0.0002
0.2
0.05
0.05
0.05
0.05
0.05
0.05
0.017
0.5
0.05
0.05
Non-urban
minimum
detectable,
/zg/rr)3
0.0003
0.0003
0.003
0.003
0.01
0.001
0.0002
0.2
0.05
0.05
0.05
0.05
0.05
0.05
0.017
0.5
0.05
0.05
ananograms/cubic meter (25°C).
For the NASN sites, the processes of weighing the filters before and after sampling as well as the
analysis for the individual elements or ions were performed by a centralized EPA Laboratory. This
centralized laboratory function was the responsibility of a group in the U.S. Public Health Service
until 1968 when the organization became part of the National Air Pollution Control Administration.
Since 1971, the laboratory function has been the responsibility of the Environmental Monitoring and
Support Laboratory, Office of Research and Development, U.S. Environmental Protection Agency,
Research Triangle Park, N.C. In 1973 and 1974, the processes of weighing the filters before and after
sampling were decentralized to the 10 EPA regional laboratories, but the analysis for the individual
elements or ions has been retained by the Environmental Monitoring and Support Laboratory,
Research Triangle Park. The filters were changed and flow rates recorded at the sampling locations by
State or local agency personnel or private individuals. The central laboratory analyzed the filters by
analytical procedures as identified by the analysis method. The analysis is performed by extracting
the pollutants from a portion of the filter and instumentally determining the amount of each pollutant
in the extraction. The analysis method and code assigned were based on the complete analytical
procedure, which includes the extraction of the pollutants from the filter and the determination of the
quantity of each pollutant in the extraction. Portions of individual filters are extracted and analyzed to
produce approximately 26 individual 24-hour observations per year, or portions of individual filters
are combined for extraction and analysis to create a composite sample for a month or a quarter.
I-3
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DESCRIPTION OF DATA TABLES
This publication contains a data section for each pollutant and these data sections are arranged
in the same order as the pollutants listed in Table 1. Also, for each pollutant the method of analysis
is utilized to sort the data. Within pollutant and method of analysis, the data are sorted by State site
and year.
For each individual page, the heading includes pollutant name, method of collection and analysis
the measurement units for the data, and the time period included. The standard units for all pollu-
cubTc met^ug/m'^' Wh'Ch " QiV6n '" nan°9rams Per cubic ™ter (ng/m>). are micrograms per
Table 2. SAROAD CONTACT OFFICES
Location
EPA Region I
60 Westview Street
Lexington, MA 02173
EPA Region II
26 Federal Plaza
New York, NY 10007
EPA Region III
6th and Walnut Streets
Philadelphia, PA 19106
EPA Region IV
345 Courtland Street, NE
Atlanta, GA 30308
EPA Region V
230 S. Dearborn
Chicago, IL 60604
EPA Region VI
1201 Elm Street
Dallas, TX 75270
EPA Region VII
1735 Baltimore Avenue
Kansas City, MO 64108
EPA Region VIII
1860 Lincoln Street
Denver, CO 80203
EPA Region IX
215 Fremont Street
San Francisco, CA 94105
EPA Region X
12006th Avenue (M/S413)
Seattle, WA 98101
National Air Data Branch
Chief, Requests & Information Section
Research Triangle Park, NC 27711
Commercial
telephone
(617)861-6700
(212)264-9802
(215)597-9860
(404)881-2864
(312)353-1447
(214)749-3971
(816)374-3791
(303)837-2226
(415)556-2270
(206)442-1580
(919)541-5395
FTS
telephone
223-2100
264-9800
597-8133
257-2864
353-2303
749-7126
758-3791
327-2226
556-2326
399-1580
629-5395
1-4
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The State name appears at the beginning of the data for each state and after the page heading for
each page. For each line of the report, the following data items are included: site code, city or county
name, site address, agency/project codes, sampling interval, year, number of observations, maxi-
mum value, and arithmetic mean. Information2 in addition to the site code, city or county name, and
site address is available to locate the sites. The Agency Type Code (Table 3) indicates the type of
agency responsible for the laboratory analysis, and the Project Code (Table 4) indicates the type of
surveillance being conducted. The sampling interval indicates whether the data values represent
analysis of individual high-volume filters or a composite sample containing portions of several filters.
Table 3. SAROAD AGENCY TYPES
A
B
C
D
E
F
G
H
I
J
K
L
M
N
P
Q
R
S-Y
Z
EPA Headquarters group responsible for atmospheric surveillance
EPA Headquarters group responsible for meteorological activity
EPA Headquarters group responsible for effects research
EPA Headquarters group responsible for atmospheric research
EPA Headquarters group responsible for abatement activity
State agency
County agency
City agency
District agency
Private
Institution (university, college, etc.)
Military
International agency
Other Federal nonmilitary agencies
EPA Regional Office group responsible for atmospheric surveillance
World Meteorological Organization
World Health Organization
Open for future expansion
Other
The arithmetic mean is printed in this report for data that satisfy the minimum summary criteria.
In calculating the arithmetic mean, one-half the minimum detectable value is substituted for all val-
ues less than or equal to the minimum detectable value. Reports that give the arithmetic mean even
^Directory of Air Quality Monitoring Sites Active in 1975. U.S. Environmental Protection Agency, Office of Air and
Waste Management, Office of Air Quality Planning and Standards, Research Triangle Park, North Carolina
27711, Report No. EPA-450/2-77-009, May 1977.
I-5
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LhnAU?,h the minimum summary criteria are not satisfied are available from NADB or the appropriate
EPA Regional Office. w>vpi>ai*
Summary criteria for noncontinuous observations with sampling intervals of 24 hours are:
1. Data representing quarterly periods must reflect a minimum of five observations for the quar-
ter. Should there be no measurements in 1 of the 3 months of the quarter, each remainina
month must have no less than two observations reported.
2. Data representing annual periods must reflect four valid quarters of observations that have
satisfied the quarterly criteria.
Summary criteria for noncontinuous observations with a composite sampling interval are:
1. Data for quarterly composite must reflect the four individual quarters to calculate a valid
annual arithmetic mean.
2. Data for monthly composite must reflect a minimum of 8 individual months with 2 months
in each quarter to calculate a valid annual arithmetic mean.
Table 4. SAROAD PROJECT CLASSIFICATIONS
01
02
03
04
05
06
08
09
10
11-99
Population-oriented surveillance
Source-oriented ambient surveillance
Background surveillance
Complaint investigation
Special studies
Episode monitoring
Global surveillance
Duplicate sampling
Continuous Air Monitoring Program
For Federal network and future expansion
I-6
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^Upc; IJMIwrpqiTv ^Vf e.F.
PLO BC<;T r-rrirr RLOG «;?i
F'ST in?* ftup MlMM Sf
DPI CrnpnMTF.
n. "7
0.03
MIS^ISIIPPI
?M7*oanz jKK*;nM
P.P3I
n.p?7
HISS1HRT
?62l"non7 Ki*»iSft«i CITY
,M7 L«C"*T
n.l 1
P.pt
M(1M?7oS7n001 GLftCI" NAT "*Pr
COM-FIU "LUC, l«nl Lnc,rY
7R
71
P, n?
".*?
* . HOB
235
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SITE COIF.
WY1"f NG
•i"3flftnnni VFLLovSTpNf *JHT PiR*
^^n^JCOO? CHA"»t1TTF iwlLlp
S^OI70^3^ ST. CRnT*
]9'J
«?!TF *r^n(?FS^
n . P F
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n.n?
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r-2 CnMpn*; i TF 7^
243
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1971 TO !»?<;
A*Y/ SA»PLl»'G NO. OF M4ylMUM
PROJ fMTFRVtL YP ORS, VALU?
0.001
n.not
o.noi
".noi
".000
p. ooo
o.non
n.noo
o.nni
0,001
H4RPY TR""UM AJRPHRT
260
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POLLUTANT:
•JON-C'lTFOT * Pni.LUTAMT t»rp0pT
MPTWin; Mf-Vni EMISSION SPFCTPA (LOW TTMP A
1971 TO |97<;
«?*f PI. I MS
! w T f ff V A L
APtTUMFTir
MF1N
r>3Pt»it0001 •< A P. I COP ft CO
PHOENIX
PHCE!"lir
moAnnoo^ PHnFMjx
n3o7«no01 SCnTTSOlLE
i?3nn 5n"TH ELLSWORTH PO
ro HLTM ^FPT ^L^P »R?<; F
fi^l ?^ HOMO
Ant ?v HPMR
fin i ?•* HPijp
^ni ^u Hni|p
P. !
n.l
n. i
n.i
n.i
n.i
n.i
n.i
n. i
".I
266
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NO. nf
ftpT TM«FTIr
. 10
.79
0.17
". 22
n. «n
i .ne
269
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POI LUTAMT: a"M"Ml'jM ION
MTTHnO: HJ-VO
1 9? t TO i
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UNITS: I'G/<"" TTFR ( ?5 ci
P*U IJT6MT! SML' ATF IP*'
,,,,B«rnn| '.JJJjj^ NFAlTHFeF«Tr!rii-» HFPPFRHA «n| ft B«,JB 7| 21
73 '
71 1"
71 21
71 30
71 30
71 30
71 73
711 2*
71 27
71 13
71 25
71 1*
71 75
71 7?
71 ?*
70 77
f 1 1 •*
7" *
71 *
7* 9
Ht.Nir.Ht IHIILnlMfi 1-1 W *P1 71 HPU" 71 ?S
71 »s
71 1*
„ ,,T.Hr MOTrL 707 (•*»» AV «"l »1 H""" " "
71 1*
71 15
71 13
71 ?7
71 «
71 71
Tl* 17
71 Z"
71 23
*HP"I* Tft c flll -»1 HIilR 71 27
71 29
ftfll 71 Hni|B 79 2*
71 1'
1,720007" 0
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1971 TO 1 97^
STATF cpOF Apfrft MTF ADDRESS
TE '«"?ipP01 N&SHVILLF tD* SOU™ l7™ ST n l°CKF
M«.?5^0n05 MASHV LLE CORNFR OF 16TH AVENUF MOP
itZ^noil NAqHvillE 1 G ' "» TR!*'!TY LAMP
H«j5«inni7 "ACHVHLE: 330R Kiw,* LAMP
MH?i=7C<-C[ FTP R^NK1 *31« HAYTPM BLVHi.
Ue5"o°P2 !>«» Ot'N P"R* 5T"rFT U"FP ""FP
«ip17rrol "AY n «• 7200 P«Y>'AY
,','^BSnnr! CM«MB »<; Cn EIRE STA FH Hc5 «T 23^1
nspuppn? CHAP» B<; Cn F1RF STATinN IBT PFLU1FW1
i^nisnco? cturr crrv mo H«RSFTT FIRF ST«T,ON
,,t.|COOOI CORPUS rHR,sT! VECTOR CO^TOOL 3n»l "PPS«
leiiTppni DFFP PtPK DFEp P«R',I3C1 CFMTEP
1117TO'17 FI Fan T1LLH«N Hr«LT« CFNTEP ?2n
^i-qpp..^, r,iLVFSTn*J C1TYHALL
,^ ,?noo, HAPMKSF" H»PL!NC,E»i WATER fORKS
n^'AOfO? HOI STn» KH "1 CA>I JACl'ITO
*C,W
1 1
3
1 1
3
5
cpl ?1 HnuP 2
a I
C,ol 71 HOUR 7
3 5
a 12
* 10
001 71 HOIJP 7 7
1 t 1
5 1 7
3 1
17
7 "
Knl 71 HOUR 7 '
7 «
7 1!
7 U
pol ?1 HOUR 7 3
7
7 <
73 •
7M It
7?
71
71 1
75 1
r,ol 7.1 HOUR 77
73
71 1
7^ 1
C(M 21 HOU» 71 33
73 33
71 31
1
FO 71HOUR 71
Ff 71 HDLJR 7 1
rr> ? HHuR 71
EO 7 H^UP 71
re 7 HOUR 7
EO 7 HOUR 71
Efl 7 HOUR 71
ff ? HPI'P 71
Fo ? HOUP 71
FO 7 HOUR 71
KP 7 HCMIP 71
HO 7 HOUP 71 3
G 7 H 0 u R 71
H 7 HOUR 7(
E ? HOUP 71
F 7 HOUR 71
N 7 HOUP 71 1
H 71 HOUR 71 7
H 7« HOUP 7! 3
H 711 HOUP 71 3
Cl
MAXIMUM
IS. 1
20.2
17.7
11.7
71.5
77.5
in. R
!?.«
11.9
13. S
13.3
20.5
11.2
B . fl
27.0
11 ,S
H.7
11.7
?! .2
15. ft
7?. 9
I!.S
IT. 6
?l .5
21 .1
7E1.7
17.3
17.8
21. i
in. 2
5.9
27.2
13.2
11.1
?5.8
70.7
27.8
) 15.5
1 1 .A
71.9
3 10.7
1 39.9
f 37.2
3 77.1
2 (,3.0
7 30. i
1 39.5
7 ?R . 1
ft. 7
2.9
7. ft
7.3
2.0
1 .9
6.7
3.5
U.I
6.2
9.5
23.5
71 .1
77.1
ARITHMETIC
MEAN
10.3
11.5
9.5
9.3
11. 1
11.0
9.2
343
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TECHNICAL REPORT DATA
(Please read Instructions on the reverse before completing)
REPORT NO
EPA-450/2-78-001
TITLE AND SUBTITLE
Air Quality Data For Non-Criteria Pollutants
1971 Through 1975
5 REPORT DATE
January 1978
6. PERFORMING ORGANIZATION CODE
AUTHOR(S)
National Air Data Branch
<8. PERFORMING ORGANIZATION REPORT NO.
PERFORMING ORGANIZATION NAME AND ADDRESS
U.S. Environmental Protection Agency
Office of Air Quality Planning and Standards
Monitoring and Data Analysis Division
Research Triangle Park, North Carolina 27711
10. PROGRAM ELEMEI*
11. CONTRACT/GRANT NO.
2 SPONSORING AGENCY NAME AND ADDRESS
U.S. Environmental Protection Agency
Office of Air and Waste Management
Office of Air Quality Planning and Standards
Research Triangle Park, North Carolina 27711
13 TYPE OF REPORT AND PERIOD COVERED
Final 1971-1975
14. SPONSORING AGENCY CODE
5. SUPPLEMENTARY NOTES
6. ABSTRACT
This report presents a comprehensive inventory of data produced by analysis
of hi-vol filters for trace metals and inorganic ions for 1971-1975. This in-
ventory is based on data acquired through extensive monitoring activities con-
ducted by Federal, State, and local pollution control agencies and submitted
to the U.S. Environmental Protection Agency's National Aerometric Data Bank.
KEY WORDS AND DOCUMENT ANALYSIS
DESCRIPTORS
b.IDENTIFIERS/OPEN ENDED TERMS
c. COSATI Field/Group
Air Pollution
Monitors
National Air Sampling Network
Inorganic ions
Metals
13 DISTRIBUTION STATEMENT
Release Unlimited
19. SECURITY CLASS (This Report)
Unclassified
>1. NO. OF PAGES
360
20. SECURITY CLASS (This page)
Unclassified
22. PRICE
EPA Form 2220-1 (9-73)
"3T
.S. GOVERNMENT PRINTING OFFICE: 1978-740 - 249/ 417 REGIONNO.4
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