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TABLE 3. DETECTION LIHITS OBTAINED FROM METHOD RANGE STUDY
Lower limit of
linear range
Analyte M9/L
Acetone
Acrolein
Acrylonitrile
Allyl chloride
Benzene
Bis-(2-chloroethyl) ether
Bromobenzene
Bromod i chl oromethane
Bromomethane
2-Butanone
n-Butyl benzene
sec-Butyl benzene
tert-Butyl benzene
Carbon disulfide
Carbon tetrachloride
Chlorobenzene
2-Chloro-l,3-butadiene
Chlorodibromomethane
Chloroethane
2-Chloroethyl ethyl ether
Chloroform
1-Chlorohexane
Chloromethane
2-Chlorotoluene
4-Chlorotoluene
l,2-Dibromo-3-chloroprepane
1,2-Dibromoethane
Dibromomethane
1,2-Dichlorobenzene
1,3-Dichlorobenzene
1,4-Dichlorobenzene
trans-1 ,4-Dichloro-2-butene
Di chl orodi f 1 uoromethane
1,1-Dichloroethane
1,2-Dichloroethane
1 , 1 -Di chl oroethene
cis-l,2-Dichloroethene
trans-1 , 2-Di chl oroethene
Di chl oromethane
1, 2-Di chl oropropane
170
100
170
10
3.0
55
3.0
3.0
5.5
100
1.0
1.0
1.0
3.0
3.0
3.0
5.5
3.0
30
30
3.0
3.0
30
3.0
3.0
10
3.0
3.0
3.0
3.0
3.0
170
5.5
5.5
5.5
5.5
5.5
5.5
5.5
5.5
Empirical Calculated
EDL MDL
M9/L M9/L
170
55
170
5.5
3.0
55
3.0
3.0
5.5
30
1.0
1.0
1.0
3.0
3.0
3.0
5.5
3.0
17
30
3.0
3.0
17
3.0
3.0
10 >
3.0
3.0
3.0
3.0
3.0
55
5.5
5.5
5.5
5.5
5.5
5.5
5.5
5.5
200
10
40
2
0.2
10
0.7
0.2
2
10
0.4
0.4
0.8
0.3
0.2
0.3
2
0.2
5
9
0.1
0.1
10
0.3
0.3
2
0.2
0.2
0.5
0.4
0.5
30
1
0.7
0.4
1
1
0.7
0.8
0.7
Nondetect
Cone.
W/La
100
30
100
3.0
1.0
30
1.0
1.0
3.0
10
0.3
0.3
0.3
1.0
1.0
1.0
3.0
1.0
10
10
1.0
1.0
10
1.0
1.0
5.5
1.0
1.0
1.0
1.0
1.0
30
3.0
3.0
3.0
3.0
3.0
3.0
3.0
3.0
(continued)
25
-------
TABLE 3.
Lower limit of
linear range
Analyte pg/L
1,3-Dichloropropane
1,1-Dichloropropene
cis-l,3-Dichl oropropene
trans-l,3-Dichloropropene
l.?-Dimethylbenzene
"etlv'jenzene
iir.j , methacrylate
Ethyl benzene
Hexachlorobutadiene
Hexachloroethane
Hexachloropropene
2-Hexanone
lodomethane
Isopropyl benzene
p-Isopropyltoluene
Methacrylonitrile
Methyl methacrylate
4-Methyl -2-pentanone
Naphthalene
Propionitrile
n-Propylbenzene
Styrene
1,1,1 , 2-Tetrachloroethane
1 , 1 ,2, 2-Tetrachloroethane
Tetrachloroethene
Toluene
Tr-ibromomethane
1,2,4-Trichlorobenzene
1,1,1-Trichloroethane
1,1,2-Trichloroethane
Trichloroethene
Tr i chl orof 1 uoromethane
1,2,3-Trichloropropane
1,2, 4 -Tri methyl benzene
1 ,3, 5-Trimethylbenzene
Vinyl acetate
Vinyl chloride
3.0
5.5
5.5
5.5
1.0
10
10
1.0
3.0
5.5
170
30
5.5
3.0
10
30
30
30
3.0
170
1.0
3.0
3.0
5.5
3.0
3.0
3.0
3.0
3.0
5.5
3.0
30
17
3.0
3.0
55
5.5
Empirical
EDL
M9/L
3.0
5.5
5.5
5.5
1.0
1.0
10
1.0
3.0
5.5
170
30
5.5
3.0
10
30
30
30
3.0
170
1.0
3.0
3.0
5.5
3.0
3.0
3.0
3.0
3.0
5.5
3.0
30
17
3.0
3.0
55
5.5
Calculated
HDL
M9/L
0.3
0.5
0.9
1
0.2
0.6
7
0.4
0.7
2
50
6
2
0.4
0.7
9
5
6
0.5
40
0.2
0.4
0.2
1
0.2
0.2
0.3
0.3
0.2
0.3
0.1
10
2
1
0.3
4
0.6
Nondetect
Cone.
W/La
1.0
3.0
3.0
3.0
0.3
0.3
3.0
0.3
1.0
3.0
100
17
3.0
0.3
5.5
17
3.0
17
1.0
100
0.3
1.0
1.0
3.0
1.0
0.3
1.0
1.0
1.0
3.0
0.3
17
10
1.0
1.0
30
3.0
aNondetect concentration
not detected.
the highest concentration studied at which the analyte was
26
-------
TABLE 4. ACCURACY AND PRECISION OF ANALYTE* MEASUREMENTS
IN SPIKED AND UNSPIKED SAMPLES
POTW Sludge Leachate
Water With Fulvlc Acid
Unsoiked
Spike Concentration1*
High Low High Low
Meas. Cone. Bias
Analvte (*q/L)
Acroleinc
Acrylonitrile0
Ally! chloride
Benzene 7.5
Bis-(2-chlorgethyl) etherc
Bromobenzene" 1.9
Bromodichloromethane
Bromomethaned
2-Butanonec
n- Butyl benzene" Trace
sec-Butyl benzene^ 6.2
tert-Butylbenzene° Trace
Carbon disulfide
Carbon tetrachloride
Chlorobenzene 7.1
Chi orodi bromomethane
Chloroethane6
2-Chloroethyl ethyl ether0
Chloroform
1-Chlorohexane
Chloromethane
2-Chlorotoluened
4-Chlorotoluene
1,2-Dibromoethane
Di bromomethane
1 , 2-Dibromo-3-chloropropane
1,2-Dichlorobenzene
1,3-Dichlorobenzene Trace
1,4-Dichlorobenzene 1.7
Dichl orodi fluoromethane" 7.1
1,1-Dichloroethane
1,2-Dichloroethane
1,1-Dichloroethene
cis-1 ,2-Dichloroethene
trans- 1,2-Dichloroethene
Di Chloromethane 6.0
1,2-Dichloropropane
1 , 3-Dichloropropane
1,1-Dichloropropene
cis-1, 3-Dichloropropene 3.7
,% Bias
(RSD)
-1 (12)
12 (8)
-1 (30)
12 (4)
0 (6)
48 (3)
17 (3)
62 (38)
-5 (7)
20 (4)
-1 (5)
-5 (3)
16 (11)
H (5)
26 (3)
13 (4)
32 (39)
30 (8)
26 (7)
20 (4)
28 (23)
26 (4)
29 (4)
5 (5)
11 (5)
17 (5)
12 (3)
20 (3)
18 (2)
30 (55)
22 (7)
1 (5)
10 (10)
20 (7)
20 (9)
16 (8)
26 (13)
4 (4)
6 (6)
22 (4)
,% Bias
(RSD)
0 (7) -
-2 (12)
22 (8)
3 (6)
2 (10) -
-17 (4)
-1 (3)
37 (14)
-11 (25)
0 (5)
-33 (5)
-5 (3)
16 (10)
1 (6)
3 (2)
-7 (7)
38 (11)
-18 (10)
10 (4)
0 (9)
34 (22)
59 (9)
3 (5)
-4 (4)
-1 (4)
,% Bias
(RSD)
10 (12)
6 (8)
24 (8)
25 (3)
H (10)
65 (4)
26 (2)
81 (10)
-9 (6)
49 (6)
35 (4)
20 (5)
28 (8)
22 (2)
35 (3)
13 (4)
93 (11)
,*
(RSD)
15 (5)
-7 (4)
20 (10)
4 (6)
3 (10)
-4 (6)
2 (3)
50 (10)
-5 (8)
3 (3)
2 (2)
-4 (2)
13 (5)
13 (3)
4 (2)
-1 (7)
23 (23)
25 (13) -22 (15)
27 (5)
32 (3)
2 (7)
21 (29)
36 (4)
5 (5)
13 (3)
-5 (12) -18 (9)
0 (4)
-2 (3)
2 (3)
64 (24)
19 (8)
-3 (2)
15 (13)
5 (6)
10 (8)
67 (4)
5 (6)
-5 (4)
2 (7)
-22 (3)
21 (4)
32 (4)
33 (4)
3 (20)
27 (9)
9 (4)
14 (11)
26 (7)
33 (8)
15 (8)
18 (2)
8 (4)
22 (3)
27 (4)
19 (6)
7 (8)
33 (23)
3 (3)
6 (3)
-4 (6)
-1 (4)
-7 (17)
1 (5)
2 (3)
4 (4)
33 (35)
19 (10)
-1 (7)
22 (10)
14 (3)
12 (6)
22 (4)
8 (3)
1 (6)
11 (4)
-1 (2)
(continued)
27
-------
TABLE 4. ACCURACY AND PRECISION OF ANALYTE' MEASUREMENTS
IN SPIKED AND UNSPIKED SAMPLES
POTVI Sludoe Leachate
Water With Fulvic Add
Analvte
Unsplked
Meas. Cone.
Spike Concentration1*
High Low High Low
Bias,* Bias,* 8ias,% Bias,*
(RSD) (RSD) (RSD) (RSD)
trans-1,3-Dichloropropene
trans-1,4-Dichloro-2-butenec,d
1,2-Dimethylbenzene
1,4-Dimethyl benzene
Ethyl methacrylatec,d
Ethyl benzene
Hexachlorobutadiene
Hexachloroethane
Hexachloropropenec
2-Hexanonefc
lodomethane
Isopropylbenzene
p-Isopropyltoluene
Methacrylonitrile0
Methyl methacrylatec
4-Methyl-2-pentanonec,d
Naphthalene
Propionitrilec
n-Propylbenzened
Styrene
1,1,1,2-Tetrachloroethane
1,1,2,2-Tetrachloroethane
Tetrachloroethene
Toluene
Tribromomethane
1,2,4-Trichlorobenzene
1,1,1-Trichloroethane
1,1,2-Trichloroethane
Trichloroethene
1,2,3-Trichloropropane
1,2,4-Trimethylbenzene
1,3,5-Trimethylbenzene
Vinyl acetate0
Vinyl chloride
Mean
4.4
13
Trace
Trace
Trace
Trace
Trace
Trace
2.8
1.2
19
1.4
20 (5)
72 (15)
22 (2)
9 (3)
-6 (3)
62 (4)
5 (12)
60 (6)
83 (5)
36 (24)
10 (9)
26 (2)
10 (3)
-55 (55)
34 (6)
-24 (51)
-8 (7)
-3 (9)
22 (2)
29 (3)
43 (2)
-8 (6)
15 (4)
33 (2)
11 (5)
5 (4)
7 (5)
5 (5)
9 (3)
5 (5)
36 (3)
-13 (5)
-29 (29)
26 (52)
-8 (4)
-52 (14)
0 (4)
3 (3)
-24 (4)
19 (4)
7 (14)
3 (4)
-46 (40)
-14 (8)
12 (4)
1 (4)
-2 (3)
-16 (8)
-18 (6)
-47 (5)
44 (8)
-6 (12)
10 (3)
-3 (3)
-2 (3)
-7 (5)
-4 (6;
8 (2;
-11 (8)
7 (6)
7 (6)
-7 (4)
9 (3)
-5 (6)
56 (4)
8 (3)
-1 (5)
26 (12)
16 (10)
23 (5)
50 (13)
30 (4)
20 (4)
7 (4)
77 (4)
23 (12)
60 (6)
92 (8)
2 (12)
20 (11)
51 (4)
34 (5)
11 (6)
39 (11)
15 (12)
-5 (7)
-2 (8)
57 (4)
36 (4)
48 (3)
-5 (9)
25 (5)
37 (4)
8 (6)
15 (5)
14 (3)
8 (5)
20 (2)
4 (7)
56 (4)
59 (19)
19 (6)
-6 (10)
-9 (7)
-59 (15)
4_(3)
13 (3)
-27 (10)
4 (2)
4 (10)
0 (7)
-9 (19)
-18 (13)
15 (5)
0 (3)
0 (3)
-5 (5)
-17 (10)
-16 (10)
-2 (10)
-6 (5)
-5 (2)
-4 (5)
-1 (3)
-7 (8)
1 (1)
5 (3)
-10 (11)
3 (7)
21 (3)
0 (8)
12 (3)
-8 (9)
0 (2)
2 (2)
-5 (4)
33 (7)
3 (7) 25 (7) 3 (7)
aData for acetone, 2-chloro-l,3-butadiene, and trichlorofluoromethane not
included, because those compounds did not have acceptable linear ranges.
bExcept for poorly purged analytes, high concentration was 200 ug/L, and low
concentration was 20 ug/L. For poorly purged compounds, high concentration
was 2000 ug/L, and low concentration was 200 ug/L. cPoorly purged compound.
"High concentration outside of linear range. 6Low concentration outside of
linear range.
28
-------
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31
-------
APPENDIX A
CALIBRATION CURVES FROM METHOD RANGE STUDIES
-------
Acetone
JC
o
a
11 -
10 -
9 -
8 -
7 -
6 -
5 -
4 -
3 -
2 -
1 -
0 -
2 4
(Thousands)
Anolyte Concentration (ug/L)
Acrolein
5 -
a
o
H
a
u
3 -
2 -
1 -
2000 4000
Arolyte Concentration (ug/L)
A-lo*
6000
-------
Acrylonitrile
Jt
a
a!
o
>
c
a:
12
11 -
10 -
9 -
8 -
7 -
6 -
5 -
4 -
2 4
(Thousands)
Analyte Concentration (ug/L)
Allyl chloride
JC
o
o
o
-------
JC
o
0.
a
7 -
6 -
5 -
4 -
Benzene
2 -
200 400
Analyte Concentration (ug/L)
600
Bis(2chloroethyl)ether
JC
a
a
d
2.8
2.6 -
2.4 -
2.2 -
2 -
1.8 -
1.6 -
1.4 -
1.2 -
1 -
0,8 -
06 -
0.4 -
0.2 -
0
2 4
(Thousands)
Analyte Concentration (ug/L)
A-3
-------
Bromobenzene
a
a
>
IP
a
a
IE
1 -
40 60 80 100 120 140
Analyte Concentration (ug/L)
160
Bromodichloromethane
1
n
c
a
o
o
200 400
Analyie Concentration (ug/L)
A-4
600
-------
Bromomethane
1
a
5
P
o
o
1C
11
10 -
9 -
8 -
7 -
6 -
5 -
4- -
3 -
2 -
1 -
0
200 400
Analyte Concentration (ug/L)
600
2Butanone
4 H
O
O
n
o
c
IT
2 4
1 4
2 4
(Thousands)
Anolyte Concentration (ug/L)
A-5
-------
J£
a
a.
nButylbenzene
60 80 100
Analyte Concentration (ug/L)
120
140
160
a
a
a.
y
a
c
secButylbenzene
40
60 80 100
Analyte Concentration (ug/L)
A-6
120
140
160
-------
11
Jt
o
o
0.
_
a
tertButylbenzene
40 60 80 100 120
Arvolyte Concentration (ug/L)
140
160
Carbon disulfide
JC
o
41
a.
a
o
a:
200 400
Anolyte Concentration (ug/L)
A-7
600
-------
Carbon tetrachloride
JC
o
s.
o
a
5 -
4 -
3 -
2 -
1 -
8
200 400
Analyte Concentration (ug/L)
600
Chlorobenzene
JC
a
n
D
160 200
Analyte Concentration (ug/L)
A-8
240
280
-------
2Chloro 1,3butadiene
a
o.
o
v.
1.5
1.4 -
1.3 -
1.2 -
1.1 -
1 -
0.9 -
0.8 -
0.7 -
0.6 -
0.5 -
0.4 -
0.3 -
0.2 -
0.1
200 400
Analyte Concentration (ug/L)
600
a
o
CL
_
a
o
or
1 -
Chlorodibromomethane
200
400
600
Concentration (ug/L)
A-9
-------
Chloroethane
0.
I
o
X.
5 -
4.5 -
4 -
3.5 -
3 -
2.5 -
2 -
1.5 -
1 -
0.5 -
0 -
200 400
Analyte Concentration (ug/L)
600
a
o
a
§
2-Chloroethyl ethyl ether
0.8
1.2 1.6
CTSouaands)
Analyte Concentration (ug/L)
A-10
2.4
2.8
-------
Chloroform
o
0.
a
32
30 -
28 -
26 -
2* -
22 -
20 -
18 -
ie -
14 -
12 -
10 -
8 -
6 -
4 -
2 -
0
200 400
Analyte Concentration (ug/L)
600
1-Chlorohexane
a
a
d
o
c
(t
200 400
Analyte Concentration (ug/L)
A-11
600
-------
Chloromethone
Jt
a
a
a
a
IE
5 -
4.5 -
4 -
3.5 -
3 -
2.3 -
2 -
1.5 -
1 -
200 400
Analyte Concentration (ug/l_)
600
2-Chlorotoluene
a
o
a.
_
0
o
200 400
Analyte Concentration (ug/L)
A-12
600
-------
4Chlorotoluene
e
«
a
o
a
K
400
600
Analyte Concentration (ug/L)
1,2 Dibromo3chloropropane
JC
a
H
o
P
o
I)
IT
1.3
1.2 -
1.1 -
1 -
0.9 -
0.8 -
0.7 -
0.6 -
0.5 -
0.4 -
0.3 -
0.2 -
0.1 -
0
s
200 400
Analyte Concentration (og/L)
A-13
600
-------
1,2Dibromoethane
JC
a
7
o
200 400
Concentration (ug/L)
600
Dibromomethane
JC
a
e
1
o
P
o
o
a:
200 400
Anatyte Concentration (ug/L)
A-14
600
-------
1,2Dichlorobenzene
e
a
«
E
40 80 120 160 200
Analyte Concentration (ug/L)
2+0
280
1,3Dichlorobenzene
JC
a
o
H
I
o
o
IT
160
Arxjlyte Concentration (ug/L)
A-15
240
280
-------
1,4 Dichlorobenzene
JC
o
a
a:
40
80 120 160
Analyte Concentration (ug/L)
280
JC
a
o
H
trans1,4Dichloro2butene
0.9
(Thousands)
Analyte Concentration (ug/L)
A-1G
1,1
1.3
1.5
1,7
-------
Dichlorodlfluoromethane
o
Q.
5
o
a
2.3
2.2 J
2.1 -
2 -
1,9 -
1.8 -
1.7 -
1.6-
1.5-
1.4 -
1.3 -
1.2 -
1,1 -
1 -
0.9 -
0.8 -
0.7 -
0,6 -
0.5 -
0.4 -
0.3 -
0.2 -
0.1
a
a
B
20 40
Anolyte Concentration (ug/L)
60
1,1 Dichloroethane
JC
a
s.
a
o
a:
200
Analyte Concentration (ug/L)
A-17
400
600
-------
1,2Dichloroethcme
3.S -
JC
o
0.
o
_
o
2.6 -
2 -
1.5 -
1 -
0.5 -
200 400
Analyte Concentration (ug/L)
600
1,1 Dichloroethene
a
o
a
D
>
200 400
Analyte Concentration (ug/L)
A-18
600
-------
cis1,2Dichloroethene
16
15 -
14 -
13 -
12 -
11 -
10 -
9 -
8 -
7 -
6 -
5 -
4 -
3 -
2 -
1 -
0
200 400
Analyte Concentration (ug/L)
600
trans 1,2Dichloroethene
JC
a
a
V
>
t5
o
7j
IE
14 -
13 -
12 -
11 -
10 -
9 -
8 -
7 -
6 -
5 -
4 -
3 -
2 -
1 -
0
.4"
200 400
Analyte Concentration (ug/L)
A-19
600
-------
Dichloromethane
o
e
200 400
Analyte Concentration (ug/L)
600
1,2 Dichloropropane
JC
a
a
a.
o
o
E
200
Analyte Concentration (ug/L)
A-20
400
600
-------
J£
a
a.
s
a
1 -i
1,3Dichloropropane
200 400
Anolyte Concentration (ug/L)
600
1,1 Dichloropropene
JC
a
o
a.
200 400
Analyte Concentration (ug/L)
A-21
600
-------
cis 1,3Dichloropropene
JC
a
o
It
5 -
4 -
2 -
1 -
200 400
Analyte Concentration (ug/L)
600
trans1,3Dichloropropene
a
o
a
200 400
Analyte Concentration (ug/L)
A-22
600
-------
1,2-Dimethylbenzene
JC
o
o
a.
o
a:
200 400
Analyte Concentration (ug/L)
600
1,4Dimethylbenzene
3.5 -
J -
Jt
o
Q.
«
>
a
IT
2.5 -
2 -
1 5 -
05 -
200
Analyte Concentration (ug/L)
A-23
i
400
600
-------
Ethyl methacrylate
JC
a
9
o
s.
G -
5 -
4 -
3 -
2 -
1 -
0.2
0.4 0.6
(Thousands)
Analyte Concentration (ug/L)
Ethylbenzene
JE
a
o
H
o
cc.
200 400
Analyte Concentration (ug/L)
A-24
600
-------
Hexachlorobutadiene
-X
o
3
S.
4.5
40 00 120 160 200
Analyi* Concentration (ug/L)
240
280
Hexachloroethane
a
o
H
7 -
6 -
5 -
4 -
,t
200
Anolyte Concentration (uq/L)
A-25
400
600
-------
Hexachloropropene
JC
a
2
V.
1 -
0.4
0.8
1.2 1.6
(Thousands)
Anatyte Concentration (ug/L)
2Hexanone
JC
o
41
y
o
a
a:
12 -
11 -
10 -
9 -
8 -
7 -
6 -
5 -
4 -
3 -
2 -
1 -
0
2 4
(Thousand*)
Analyte Concentration (ug/L)
A--26
B
-------
lodomethane
J4
32 -
30 -
28 -
26 -
24 -
22 -
20 -
18 -
16 -
14 -
12 -
10 -
8 -
6 -
4 -
2 -
D
200 400
Analyte Concentration (ug/L)
600
Jt
a
c
a
a
«j
a:
Isopropylbenzene
30
120 160 200
Analyte Concentration (ug/L)
A-27
240
280
-------
pIsopropyltoluene
a
c
a.
o
e
x.
SO 120 160 200
Analyte Concentration (ug/L)
240
280
Methacrylonitrile
o
(Thouaands)
Analyte Concentration (ug/L)
A-28
-------
Methyl methacrylate
a
a.
a
>
a
0.4 0.8 1.2 1.6 2
(Thousands)
Analyte Concentration (ug/L)
2.8
4Methyl2pentanone
JC
a
o
0.
o
c
0.4
0.6 0.8 1
(Thousands)
Analyte Concentration (ug/L)
A-29
1.2
1.4
1.6
-------
JC
a
5 -
4 -
2 -
1 -
Naphthalene
40 80 120 160 200
Analyte Concentration (ug/L)
240
280
Propionitrile
JC
a
a
a
o
~
3.5 -
3 -
2.5 -
2 -
1.5 -
1 -
0.5 -
2 4
(Thousands)
Analyte Concentration (ug/L)
A-30
-------
nPropylbenzene
a
a
o.
o
o
a:
20
40 60 80 100
Analyte Concentration (ug/L)
a
41
a.
u
ir
6 -
5 -
4 -
Styrene
1 -
iI i i
40 80 120 160 200
Analyte Concentration (ug/L)
A-31
240
280
-------
1,1,1,2Tetrachloroethane
I
Jf
o
I
5
80 120 160 200
Analyte Concentration (ug/L)
240
280
1,1,2,2Tetrachloroethane
JC
a
CL
a
4 -
2-
1 H
200 400
Analyte Concentration (ug/L)
A-32
600
-------
Tetrachloroethene
JC
a
a
tp
o
0
It
40 80 120 160 200
Analyte Concentration (ug/L)
240
280
Toluene
a
c
a.
o
«j
ac.
6 -
5 -
4 -
T _
2 -
200 400
Analy-te Concentration (ug/L)
600
-------
I
I
1,2,4Trichlorobenzene
40 80 120 160 200
Anolyts Concentration (ug/L.)
240
280
JC
a
CL
o
>
o
E
Tribromomethane
120
160
200
240
280
Anatyte Concentration (ug/L)
A-34
-------
1,1,1-Trichloroethcme
JC
a
a.
o
0
a:
200 400
Analyte Concentration (ug/L)
600
1,1,2Trichloroethane
JC
a
c
CL
3 -
28 -
26 -
2.4 -
2.2 -
2 -
1.8 -
1.6 -
1 4 -
1.2 -
1 -
08-
06-
04-
02-
0
200 400
Analyte Concentration (ug/L)
A-3 5
600
-------
Trichlorofluoromethane
JC
o
I
5
60
1 00 140 180
Analyte Concentration (ug/L)
220
260
300
4.5
Trichloroethene
JC
a
3
a
K.
4 -
3.5 -
3 -
1.5 -
1 -
05 -
200 400
Artalyte Concentration (ug/L)
A-36
600
-------
1,2,3 Trichloropropane
Jt
a
o
a.
1.4
1.3
1.2
1.1
1
0.9
0.8
0.7
0.6
05
0.4
03
0,2
0.1
0
200 400
Analyte Concentration (ug/L)
600
1,2,4Trimethylbenzene
D
1
Jf
a
41
Q.
4)
S
o
41
£
1 O
14 -
13 -
12 -
1 1 -
10 -
9 -
8 -
7 -
6 -
5 -
4 -
i
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j^
^>^
*>
^
^^
^*
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^S"*
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1 i 1 II!!!
'20 160 200 240 280
Arxilyte Concentration (uq/L)
A-37
-------
JC
o
o
a
3
a
c
K.
1,3,5Trimethylbenzene
40 80 120 160 200
Analyte Concentration (ug/L)
240
280
.
a
ti
0.
a
o
10 -
Vinyl acetate
0,8
1.2 1.6
(Thousands)
Analyte Concentration (ug/L)
A-38
2.4
2.8
-------
Vinyl chloride
JC
o
s.
0
IT
6 -
5 -
4 -
3 -
2 -
1 -
200 400
Anolyte Concentration (ug/L)
600
-------
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