600R81101
            GUIDELINES AND SPECIFICATIONS FOR IMPLEMENTING

                    QUALITY ASSURANCE REQUIREMENTS

           FOR DEMONSTRATION PROJECTS FINANCIAL ASSISTANCE

                 INVOLVING ENVIRONMENTAL MEASUREMENTS
                            QAMS-003/80/02
                  Quality Assurance Management Staff
          Office of Monitoring  Systems- and Quality Assurance
                  Office  of Research and Development
                 U.S.  Environmental Protection Agency
                           August 3, 1981
                  U.S. CfiVlr •       "     :->a Agency
                  ftoglon '
                  230 80s.:.
                  Chicago,  n,.»\       -jiV«
                             DRAFT

-------
              Guidelines and Specifications for Implementing
                      Quality Assurance Requirements
             for Demonstration Projects Financial Assistance
                   Involving Environmental Measurements
                                 Abstract


     On May 30, 1979, an EPA policy was  established requiring all Regional

Offices, Program Offices, EPA Laboratories, and the States to participate

in a centrally-managed Agency-wide Quality Assurance  (QA) Program.  The

stated goal of  the program  is  to ensure that  all environmentally-related

measurements which are funded  by EPA or which generate  data mandated by

EPA are  scientifically  valid,  defensible, and  of  known precision and

accuracy.  A memorandum dated  June 14, 1979 extended these  QA require-

ments to all  EPA extramural projects,  including  contracts,  interagency

agreements, and grants and cooperative agreements that  involve environ-

mental measurements.


     This document  aids  Project  Officers,  QA  Officers,  and  Program

Managers Involved in the administration of demonstration projects (grants

and cooperative agreements) to uniformly Implement the Administrator's QA

Policy.  The Intent  of this document is  to ensure that  QA  requirements

for these  extramural  projects  are  consistent  and  appropriate to meet

EPA*s data quality objectives.


     Guidance and review forms  are provided to assist in the systematic

review of QA requirements for environmental measurement projects assisted

by EPA.  The   steps  of  the review include:   (1) requirements  of the

application; (2) evaluation  of  the application;  and (3)  requirements of

the agreement.

-------
     Applicants for  assistance  should  stipulate  their willingness  to



participate in  appropriate  EPA QA  performance  audits  as  part  of  the



evaluation process  or  during  the  assistance  period.   Each  applicant



will be required  to  submit  a QA  program plan to  EPA  for  approval  and



agree to prepare a QA project  plan(s)  prior to  award of financial assis-



tance.  The QA program  plan  will become a part of the agreement incorpo-



rated by  reference.   The  agreement  must  also  include  requirements  for



submitting separate periodic QA reports,  EPA's right -to  conduct en-site



QA systems  audits,  and as  appropriate,  requirements  for  participation



in EPA performance evaluation (PE)  studies.

-------
                                                      Revision No. I
                                                      Date:  8-3-81
                                                      Page 1 of 10
              Guidelines and Specifications for Implementing
                      Quality Assurance Requirements
             For Demonstration Projects Financial Assistance
                   Involving Environmental Measurements
1.0  INTRODUCTION

     By memoranda  of May  30,  1979 and  June 14,  1979  EPA established

policy requiring participation in  a Quality  Assurance  (QA) Program by

all organizations  conducting  environmental  measurements required or  sup-

ported by the EPA.  The aim of this policy is to ensure that all environ-

mentally related measurements  funded or mandated by the EPA are scienti-

fically valid,  defensible,  and  of  adequate and   known  precision  and

accuracy.


1.1  Purpose

     The purpose of  this  document is to assist  EPA Project Officers, QA

Officers, and  Program  Managers  in  the uniform   implementation   of QA

requirements for environmental  measurements supported via Federal Assis-

tance for  Demonstration  Projects.   This  document  does  not  invalidate

&ny QA requirements stipulated in current EPA regulations.



1.2  Authority

     The Office of Research and  Development is delegated  the  responsi-

bility to develop and direct the implementation of -the National QA Program

for the  Agency (Delegation of  Authority  Manual,   Chapter  1_,  March 4,

1981).

-------
                                                      Date:  8-3-81
                                                      Page 2 of 10
1.3  Applicability and Scope

     This document applies to  all  financial assistance for Demonstration

Projects involving environmentally related measurements.   This includes

all demonstration assistance agreements designated  as  Grants or Coopera-

tive Agreements under  the Federal  Grant  and Cooperative  Agreement Act,

40 CFR Part 30.


1.4  Definitions

     .1  Applicant - any  individual, agency,  or entity which has filed a

         preapplication or an application for Federal Assistance pursuant

         to the Federal Grant and Cooperative Agreement Act.

     •2  Assistance —  an  award of funds  or  other aid  via  a  written

         assistance agreement,

     .3  Assistance Agreement - the written agreement  (grant or coopera-

         tive agreement) and amendments thereto between EPA and a recipi-

         ent in which  the terms and conditions  governing  the assistance

         are stated and  agreed to by  both parties pursuant to 40  CFR

         Part 30,  revised as of_June 30, 1978.

     .4  Assistance Approving Official  —  the  EPA  official  designated

        to approve assistance  and  take other  assistance-related actions

         authorized by Environmental Protection Agency Orders  or 40  CFR

         Part 30 (Sometime referred to as the Decision Official).

     .5  Demonstration Project - vode of assistance for demonstrating the

         practical application  of  a new  device, technique, or  control

         technology to  a process or measurement.

-------
                                                   Date:  B-ii-Bl
                                                   Page 3 of 10
  .6  Environmental Measurement -  all field or  laboratory investiga-

      tions which generate data such as measuring the chemical, physi-

      cal, or biological  parameters  in the environment;  determining

      pollutants in waste  streams;  conducting  health  and ecological

      effect studies;  carrying out clinical and  epidemiological inves-

      tigations; performing engineering and process  evaluations;  con-

      ducting studies  involving  simulation of  environmental  events;

      investigating"pollutant transport and fate;  and  developing  and

      using models.

  .7  Federal Assistance -  the  entire  Federal  contribution  for  a

      project including, but not limited to, the EPA Assistance amount.

  .8  Performance Evaluation - documentation  of laboratory's  ability

      to consistently  produce valid  data  of  known  and  acceptable

      quality.  This is done through analysis  of samples  of -known and

      certified  concentration.

 .9  Project - the undertaking identified  in the assistance agreement

      which will receive EPA assistance for a specified budget  period;

      may refer   to  a  program (e.g.,  State water  pollution  control

      program, air pollution  control program).


.10  Project Officer - the EPA official designated in  the assistance

    agreement as the Agency's  principal  contact  with the  recipient

    of  funds for  a particular project;  this person  Is  responsible

    for monitoring the  performance  and  coordinating  the project.

-------
                                                 Revision No. 1
                                                 Date:  8-3-81
                                                 Page 4 of 10
.11   Project Period - the period of time specified in the assistance

     agreement estimated to be required for completion of the project

     for which Federal assistance has been requested; it is composed

     of one or more budget periods.

.12   quality Assurance - the  total integrated program  for assuring

     the reliability of monitoring and measurement data.

.13   Quality Assurance Officer - that individual who is assigned the

     responsibility for QA overview and guidance of QA for an organi-

     zation or for a  specific project;  the QA officer must be  in a

     position to provide independent and objective  evaluations and

     assessments of the effectiveness of the QA program, and to pro-

     vide timely feedback recommendations and approvals.

.14   Quality Assurance Program Plan - a written document prepared by

     applicant/recipient which presents,  in general terms, the over-

     all policies,  organization,   objectives,  functional  responsi-

     bilities (within  the  organization),  and  general  procedures

     designed to achieve data  quality goals.

.15   Quality Assurance Project Plan - a written document prepared by

     applicant/recipient for a  specified project which  details the

     policies, organization, objectives,  functional  activities, and

     specific QA and quality  control (QC) procedures and activities

     designed to achieve data  quality goals or requirements. The QA

     project plan includes  specific procedures to be used to routinely

     assess data precision, accuracy, completeness,  representativeness,

     and comparability of the  measurements involved.

-------
                                                      Revision NO. i
                                                      Date:  8-3-81
                                                      Page 5 of 10
    .16  Quality Assurance Systems Audit - a quantitative analysis or check

         with a material or device with known properties or characteristics.

         Such audits are performed periodically to determine the accuracy of

         a measurement system.

    .17  Quality Assurance Systems Audit - a systematic on-site qualitative

         review of facilities, equipment, training, procedures, recordkeeping,

         data validation, data management,  and reporting aspects  of the

         total QA system.

         (QA plans  and  audits are  required to assess the  capability of

         the measurement  system  of  applicant  to generate  data  of  the

         required quality  or to  determine  compliance of recipient with
                i
         the QA requirements  of the  Grant or  Cooperative  Agreement*

    •18  Recipient —  any individual,  agency,  or entity  which  has been

         awarded assistance pursuant to 40 CFR 30.345.

    .19  Regional Administrator - the Administrator of one of the ten EPA

         Regional Offices  or  any  person  authorized to  act  for  him.

    .20  State-KPA Agreement  -  a statement between the  State and  EPA

         delineating priority program activities to be carried out in the

         State by  either party;  the  document  specifically covers  work

         to be undertaken during the fiscal year encompassed.



2.0  QUALITY ASSURANCE HEQUIBgMENTS


     Recipients of  Federal assistance must comply  with  QA  guidelines

     described in References 1 and 2, Appendix B.

-------
                                                      Date:  8-3-81
                                                      Page 6 of 10
3.0  QUALITY ASSURANCE REVIEW

     Recipients of  assistance  are  responsible  for the  QA requirements,

established through negotiation, for all phases of the project.  However,

EPA Project Officers and QA Officers both share responsibility for imple-

menting QA requirements in all Agency assisted environmental measurement

projects.  Tom QAE-DCA (for EPA Internal Use Only) has been prepared to

assist EPA personnel  in  evaluating QA systems  described in applications

for assistance  involving  environmental  measurements  for  demonstration

projects.


    The QA Officer  of the sponsoring  office will  notify  QA Officers of

all other offices having substantial  Interest in the assistance activity

(program, Regional  offices,  and  laboratories)  for  an opportunity  to

comment if they so desire.                                   	



3.1  Assistance Conditions

     Special conditions of  the Assistance Agreement, Tart V  of EPA Form

     5700-20A (Revision 8-79) must  include  QA requirements of the agree-

     ment.  As a m-tri-tnmm  condition of the assistance, the applicant must

     state his QA policy, ensure the preparation  of QA project plans for

     all environmental measurements (see Reference 2,  Appendix  B),  and

     agree to participate  in  relevant EPA performance evaluation  stu-

     dies.  As applicable,  the  following QA areas should  also  be ad-

     dressed in Part V.
     1.  The  intended  use of  the  data and  the associated  acceptance
         criteria for data quality

-------
                                                        K.evision no. i
                                                        Date:  8-3-81
                                                        Page 7 of 10
       2.  Project requirements for precision, accuracy, representativeness,
           completeness, and comparability

       3.  Selection of sampling sites and collection of samples

       4.  Sample identification, preservation, transportation, and storage

       5.  Selection of analytical methods

       6.  Standard QA/QC procedures to be followed.


           The procedures  to be  used for  the  above QA  areas  should be

           identified and  discussed  in  sufficient  detail  to  allow  an

           assessment of the QA practices  to be followed during the project.

           In most cases,  an in—depth and detailed discussion of -each area

           •will not be necessary at this time.  for example, *here standard

           procedures described  in  an  EPA  handbook  or  other  standard

           reference are ±o be followed, they may be included by reference.

           Sections III  through  VI  of   Form  QAR-DCA  should  be used to

           determine specific QA requirements and schedules.


3.1*1  QA System Audit

       Applicants will  be  informed  in  the  Application  Kit,  or in pre-

       application assistance,  that they  may be  required  to  permit  cm-

       site systems audits as part of the preaward evaluation or during the

       period of the performance under the agreement or both.


3.1.2  QA Performance Evaluation Studies

       Performance evaluation studies will be a part of the agreement unless

       no QC reference materials  or devices 
-------
                                                      K.BVJ.B AUIJ. nu.
                                                      Date:  8-3-81
                                                      Page 8 of 10
     In the event  that no routine QC reference  materials or devices are

     available for  the measurements  involved,  consideration  should be

     given to the  use  of  common samples  (or split samples)  for cross-

     comparison of results from the recipient with those  of EPA.


3.2  Preaward Requirements

     Prior to  formal  review  and  approval of  applications  for Federal

assistance, the  Project Officer  and QA Officer  must determine  if the

project requires  the  generation  of  environmentally-related measurement


data covered  by  the Agency's  mandatory QA policy.   If  so,  the Project

Officer must  delineate the QA requirements, approved  by  the QA Officer,

which each applicant must include in the application.  The following will

be included in the special instructions as reqirements for assistance and

will be submitted as part of the application.


     1.  A QA program plan as described in Section 3.2.1

     2.  Agreement,  if requested,  to participate in  Performance Audits
         using selected  QC reference  samples/devices or  agreement  to
         document performance on  such samples;  such reference samples or
         devices will  be  supplied  by EPA at  no cost to the recipient.

     3.  Agreement, to permit a QA systems audit by EPA  of  the applicant's/
         recipient's facilities and operation.


     Whenever appropriate, the QA Officer will ensure that the requirements

for QA project plans,  QA performance audits,  and QA  systems audits are

met by an applicant or recipient.

-------
                                                        nevjL.Dj.uu »u• j.
                                                        Date:  8-3-81
                                                        Page 9 of 10
3.2.1  QA Program Plan

       The application will include  the following information concerning the

       management of the QA effort for the proposed project:


       1.  A statement of policy concerning the  applicant's  commitment to
           implement QA procedures  and  policies  to  assure generation of
           data of known quality to meet project objectives.

      2.   An organizational structure showing the position of each key
           person associated  with the project.

      3.   A delineation of the QA authority and responsibilities of each
           key person involved in generating or processing data.


3.2.2  QA Project Plan

       The applicant nay  be required to submit, as part  of the assistance

       proposal, a proposed QA project plan for the effort required by the

       project.  If not included  as part of the assistance proposal,  a QA

       project plan must  be developed as a separate,  or  identifiable part

       of the recipient's work plan (see Section 3.3)


  3.3  Award

       In reviewing the QA requirements for assistance, the Project Officer

  will, in accordance with  Section  3.1,  delineate  the  needs of the project

  for various QA activities throughout  the duration  of the agreement.  A

  complete and detailed QA project plan will be required to be submitted as

  a deliverable item.  The  QA project plan will be approved by the Project

  Officer and QA Officer and shall  be adhered  to.  Provisions  will be made

  in the assistance agreement for formal approval of any subsequent revisions

  of the QA project plan.

-------
                                                      Revision No. 1
                                                      Date:  8-3-81
                                                      Page 10 of 10
3.4  QA Reports

     Projects of 6  months or less  may require  only  a final  QA report.

     Projects of longer duration may require periodic QA reports.  The QA

     reports will be  separately identified  progress  reports  and should

     contain such information as:

     1.  Changes to QA management

     2.  Status of completion of QA project plan

     3.  Measures of data quality from the project

     4.  Significant quality  problems,  quality accomplishments, and status
         of corrective actions

     5.  Results of QA performance audits

     6.  Results of QA system audits

     7.  Assessment  of data  quality  in terms  of precision,  accuracy,
         completeness, representativeness, and comparability

     8.  Quality-related training.

-------
                                          APPENDIX A
C
                                QUALITY ASSURANCE REVIEW FOEMS

-------
               QUALITY ASSURANCE REVIEW FOR EXTRAMURAL PROJECTS
             (DEMONSTRATION PROJECTS AND COOPERATIVE AGREEMENTS)
  I.  GENERAL INFORMATION

  1.  Descriptive Title:
  2.  Sponsoring Program Office:

  3.  Responsible Region(s)
      (where applicable)  	
  4.  Approximate Dollar Amount:

  5.  Duration:
  II.  DESCRIPTION OF WORK                                   Yes     No

       This Project requires environmental measurements?     	
                                                              Tes     No
HI.  QUALITY ASSURANCE ASSISTANCE AGREEMENT REQUIREMENTS
      (Projects requiring environmental measurements)
  1.  A written QA project plan is required as a part of
      the agreement.  (Required if the answer to II is
      yes.)
  2.  Submission of a written QA project plan is to be
      included in the assistance application.

  3.  Audit samples or devices are available for the
      parameter(s) relevant to this project (complete on
      reverse side).

  A.  Performance on available audit samples shall
      be required,  (complete on reverse side).
      If not, attach justification for exception.

  5.  An on-site evaluation of applicant's facilities
      will be made prior to -award to ensure that a QA
      system is operational and exhibits the capability
      for successful completion of this project (complete
      on reverse side).
  QA Form QAR-DCA,  Revision No.  0,  1980
                                 Page 1  of 2

-------
       Measured      Sample or Device            for          ior              miring
                       Available         Cross-Comparison    Preaward     Assistance Agreemen
                       (Yes or No)(Yes or No)(Yes or No)
      1.

      2.

      3.

     .4.

      5.

      6.

      7.

      8.

      9.

     10.
 7.  PLANNED DATES FOR QA SYSTEMS AUDITS             Planned Audit Team

     Preaward          During Agreement        	
VI.  QA REPORTS SCHEDULE

     Progress Reports ___

     Final Report
     Before submission of the application to Assistance Approving Official, the signatures
     below verify that the QA requirements have been established.

     Project Offleer/Review Panel:            Concurrence QA Officer:
     Signature                Date             Signature               Date


     After the selection of the recipient,                     . the signatures below
     verify that the preaward requirements have been satifactorily fulfilled.

     Project Officer:                          Concurrence QA Officer:
     Signature                Date             Signature               Date

     After signing, mall a copy of this form to the QAMS (RD-680) and to the
     Assistance Approving and Award Officials.

     QA Form QAR-DCA                                    "~~    ~   "  ~~   ~"~
                                              Pa-e 2 of 2

-------
 APPENDIX B
BIBLIOGRAPHY

-------
     The following EPA documents or regulations provide guidance on

establishing QA programs for environmental measurement projects for

various media or pollutants.  There are many other reference works also

available,

General

1.  Guidelines and Specifications for Preparing Quality Assurance Program

    Plans, QAMS-004-80

2.  Guidelines ans Specifications for Preparing Quality Assurance Project

    Plans, QAMS-007-80
     Air

  • A-l.  EPA-600/9-76-005

                «

  A-2.   EPA-600/4-77-027a



   A-3.  EPA-600/4-77-027b



   A-4.  EPA-600/4-76-044



   A-5.  Regulation


    Water

  ¥-1.  EPA-660/4-019



  ¥-2.  EPA-600/4-78-017
  W-3.  EPA-600/4-75-008
        HTIS-PB-253258/AS
Quality Assurance Handbook for Air Pollution
Measurement Systems.  Volume I, Principles
(March, 1976)

 Quality Assurance Handbook for Air Pollution
Measurement Systems.  Volume II, Ambient Air
Specific Methods (May, 197.7J	

Quality Assurance Handbook for Air Pollution
Measurement Systems.  Volume III, Stationary
Source Specific Methods (August, 1977)

The EPA Program for the Standardization of
Stationary Source Emission Test Methodology-
- A Review (August, 1976)

Federal Register, May 10, 1979, Appendices
A&B
Handbook for Analytical Quality Control
in Water and Wastewater Laboratories
(March, 1979)

Procedures for the Evaluation of Environmental
Monitoring Laboratories (March, 1978)

Prescribed Procedures for Measurement of
Radioactivity in Drinking Water (March, 1976)

-------
                             'M "C1
U.S. EnvJr --""•*         "^ Agency
Region v
230 Sf
Chicago,             "-'

-------
    Water (continued)

  W-4.  EPA-600/8-73-008
  W-5.  EPA-600/-78-017


  W-6.  EPA-600/4-79-020


  W-7*  EPA-600/2-79-046


  W-8.  Regulation

  W-9.  Regulation

 W-10.  Regulation
Manual for the Interim Certification of
Laboratories Involved in Analyzing Public
Drinking Water Supplies, Criteria, and
Procedures (August, 1978)

Microbiological Methods for Monitoring
and Environment (December, 1978)

Methods for Chemical Analysis of Water
and Wastes (March, 1979)

Quality Assurance Guidelines for IERL-CI
Project Officers (December, 1979)

Federal Register, December 1, 1976

Federal Register. November 29, 1979

Federal Register, December 18, 1979
   Radiation

 R-l.  EPA-600/4-78-033
       NTIS-PB-286981/AS

 R-2.  EPA-600/4-78-032
       NTIS-PB-284850/AS
 R-3.  EPA-600/7-77-088
       TVA-E-EP-77-4
       NTIS-PB-277254/9BE
Radioactivity Standards Distribution Progri
1978-1979 (June, 1978)
Environmental Radioactivity Laboratory
Intercomparison Studies Program 1978-1979
(June, 1978)

Handbook for Analytical Quality Control and
Radioactivity Analytical Laboratories
(August, 1977)
   Pesticides

 P-1-  EPA-600/1-79-008
P-2.  Environmental
      Toxicology Division,
      Health Effects
      Research Division,
      U.S. EPA, Research
      Triangle Park, NC

      EPA-600/1-013
Manual of Analytical Quality Control for
Pesticides and Related Compounds in Human
and Environmental Samples (January, 1979)

Analysis of Pesticides Residues in Human and
Environmental Samples—A Compilation of
Methods Selected for Use in Pesticide
Monitoring Programs.
Guides for Quality Assurance in
Environmental Health Research (January,
1979).

-------