United States
                  Environmental Protection
                  Agency	
Environmental
Research Laboratory
Athens. GA 30613
-

                  Research and Development
EPA/600/S3-88/007 Apr. 1988
f/EPA         Project Summary
                  Interim  Protocol  for  Measuring
                  Microbial  Transformation  Rate
                  Constants  for Suspended
                  Bacterial  Populations  in Aquatic
                  Systems
                  William C. Steen
                    An interim protocol for performing
                  research  to measure  microblal
                  degradation rates  of  organic
                  chemicals  in  freshwaters Is
                  presented. Microblal degradation is a
                  major transformation pathway
                  influencing the environmental fate of
                  chemicals. The interim  protocol
                  presented provides  a  basis  for
                  measurement   of   microblal
                  degradation rates such that reliable,
                  comparable and consistent data can
                  be obtained by different laboratories
                  and research investigations.  As
                  additional  research and information
                  Is  gathered  on  the  environmental
                  factors  affecting  microblal
                  degradation by suspended bacterial
                  populations  In freshwater, the
                  outlined protocol will be modified.
                     This Project  Summary  was
                  developed by EPA's  Environmental
                  Research Laboratory,  Athens, GA, to
                  announce key findings  of the
                  research  project that  Is fully
                  documented in a separate report of
                  the same  title (see Project Report
                  ordering Information at back).

                  Introduction
                    Under the Toxic Substances Control
                  Act of 1976 (PL 94-469), EPA's Office
                  of Toxic Substances is required to review
                  the potential risk to human health and the
                  environment posed by new  chemicals
                  before manufacture  and use  are
                  permitted. For many chemicals, microbial
 degradation is a major transformation
 pathway  that  influences  their
 environmental fate. Therefore,  in
 assessing risk, it is necessary to have
 some estimate  of  the  microbial
 transformation rate of each chemical.
   The  Office of Toxic  Substances
 estimates microbial transformation rates
 of chemicals proposed for manufacture
 by comparing  each new  chemical's
 organic  structure (or other known
 properties) with those of chemicals
 whose microbial transformation rates
 have been established.  Chemicals with
 similar structures/properties are expected
 to have similar  microbial transformation
 rates.   Unfortunately,  microbial
 transformation rates and rate constants
 have been measured for only  a few
 chemicals. Investigations are  being
 expanded,  however, as  a better
 understanding of the many environmental
 factors  that influence  microbial
 degradation is achieved. Much remains
 to be learned  about ways in  which
 population  density  and diversity,
 accessibility of chemical substrate within
 microcosms, and other factors influence
 transformation rates.
   While  these investigations continue, it
 is necessary to  provide measured
 microbial  transformation rates  for
 chemicals based on current knowledge.
 These microbial rates must be measured
 in a manner that is reproducible and that
 assures the results of measurement of
 one chemical can be compared to those

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of another with confidence, even though
the influence  of  some environmental
factors is not fully understood.
   This report represents a sampling and
measurement  protocol that has  been
applied  over  several years  at the
Environmental  Research  Laboratory,
Athens, GA.  The methodology has been
found to provide  reproducible  second-
order  rate constants  using  suspended
natural populations in  aerobic  aquatic
systems. Transformation rate is based on
the rate  of  disappearance  of  the test
chemical.
   The  interim protocol  provides  a
stepwise description  of  methods for
establishing  aerobic  biodegradation
investigations. In a typical biodegradation
study,  natural  aquatic sites  within the
vicinity of the  investigator's  laboratory
are sampled.  Water  temperature is
recorded,  and  the  samples  are
transported  to the  laboratory.  After
receipt at the  laboratory,  samples are
filtered to remove coarse debris.
   Population  densities  should  be
measured by  standard plate  counts
(heterotrophic plate  counts).  This
characterization  serves  to establish the
baseline population  density  of the
ambient water and  to determine the need
for a  concentration  procedure for
increasing population  densities  in  order
to observe  measurable  rates in the
transformation of test chemicals.
   The time lapse between sampling and
initiation   of  the  rate   constant
measurement phases  should be no more
than  12 hours.  Once the microbial
samples have  been returned  to the
laboratory, handling prior to experimental
rate constant measurement can  take two
courses.
   In one procedure, the sample is used
at the natural  population  density  when
sampled. The test chemical is added and
the chemical's transformation  rate is
measured.
   In  the alternative  procedure, the
natural microbial population is enhanced
through a concentration step. This 10:1
concentration  step  requires larger
volumes of source water.
   Bacterial populations  in water samples
are concentrated 10-fold by  filtering 10
liters through a membrane filter  (0.2 pm
pore diameter,  Nucleopore or equivalent)
that has been prewashed  with  distilled
water. After filtration, filters are placed in
a  2-liter,  wide-mouth,  cotton-plugged
Erlenmeyer flask containing 1 liter of the
original source  sample.
   Sterile, aqueous, concentrated  stock
solutions of  nutrients are  prepared to
yield concentrations (g/L) of each of the
following: NH4CI (0.5), (NH4)2SO4 (0.5),
Na2HP04 (0.5), KH2P04  (0.5), MgSO4
(0.001), and FeCIa (0.001). No more than
1 ml of  each nutrient  is added  to the
concentrated bacterial population.  These
bacterial suspensions are then incubated
for 48 hours at 22 °C in a temperature-
controlled shaker (150  to  200  rpm)
before each experiment is initiated. This
procedure  enhances  the  bacterial
population 10- to 100-fold.
   Bacterial  concentrations  are
determined by  pour plating  techniques
using Tryptone  Glucose Extract Agar
(TGE)  from serial  dilutions of  each
reaction flask.  Each  dilution is plated  in
duplicate or triplicate.  Pour  plates are
then  incubated for 48 hours at 22±1°C
in  the   temperature-controlled
incubator/shaker. Following the 48-hour
incubation, plates  are removed  and
bacteria are counted (using  a suitable
counting instrument),  tabulated,  and
arranged.
   Following preparation of  abiotic and
biotic treatment  flasks, test chemical
disappearance is  measured within each
reaction  flask  by   either  gas
chromatographic  or high  performance
liquid chromatographic  methods. Raw
data  on the test chemicals are obtained
by  measuring  the concentration  of
chemical remaining in  the reaction flask
at specific time intervals. The measured
concentration at time zero serves  as the
reference point for the remaining  points.
From these data, the first-order slope  or
rate  constant (k, hr1) is  determined
either  through  standard  laboratory
computer programs or manually through
graphical manipulations  using semi-log
paper.
   Using  the  mean  of  bacterial
concentration  determined  from  plate
counts and  first-order  slopes (k, hr1)
for  chemical  disappearance,  the
second-order rate constant  (kb, L org-1
hr1) is  calculated. The  applicable form
of the second-order  rate  expression
used throughout is:

         -ds/dt = kb[BT][ST]
where:
   kb   =   Second-order  rate  con-
            stant (L org-1  hr-1)
   [BT]  =  Measured    bacterial
            concentration (CFU or org
            per liter)
   [87]  =   Measured    substrate
            (chemical) concentration
            (mg per liter)
   The utility of this protocol has been
demonstrated  by   comparative
determinations  of  the  second-order
microbial  rate constants  of standard
reference  chemicals. Two  standar
reference chemicals, methyl  ester  <
2,4-dichloro  phenoxy  acetic acid (2,'
OME) and  propanil,  were  investigate
using natural pond water over a period <
1 year.  Second-order rate constant
ranged from 7.8 to 9.2 X  10-9  | org
hr1  for  nine  determinations  with  th
methyl ester of 2,4-D. Propanil yielde
rate constants  ranging from 1.1 to 6.4
10"11 I  org-1  hr1  for six determir
ations.  Coefficients of variation were 3
to 72% for the  methyl ester  of  2,4-
and 42 to 69% for propanil. No season;
effects were observed. Use of a standar
reference chemical  directly  aids  th
investigator in establishing his confidenc
in the protocol  measurements and allow
for  interlaboratory  comparativ
investigations  in  application  of  th
protocol.
    Several  basic assumptions serve a
the foundation for measurements  c
microbial transformation rate  constant
under this  protocol. Use  of total  viabl
plate count  as a measure of  microbii
population  concentrations provides
measurement  that  is  assumed to b
proportional  to  the   number  c
microorganisms  participating  in  th
biodegradation process. For chemical
for which the concept was developed  an
tested,  many  of  the  culturabl
populations  indigenous  to  aquati
systems  support  the  necessar
constitutive enzymes for microbiall
mediated  hydrolysis and  oxidatio
reactions.  Moreover, the transform
ation/biodegradation process is  pseudc
first-order  with respect to bacterie
concentration  and, therefore,  i
proportional to the density of total viabl
bacteria in the system plated on TGE.
is further assumed that the substrate (tes
chemical) concentration  is  much les
than the theoretical Ks  half-saturatio
concentration and that reaction kinetic
are first-order  with respect to  substrat
concentration.  It also is  assumed  the
carbon and energy contributions from th
chemical  under investigation  are  nc
sufficient to cause measurable growth t
the  constitutive   populations.  Th
second-order mathematical descriptio
of  biodegradation  serves   as
reproducible and reliable measurement c
microbial transformation rate  constant
for organic  chemicals in aquatic system;

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  The EPA Author,  William  C. Steen,  (also the Project  Officer)  is with  the
       Environmental Research Laboratory, Athens GA 30613.
  The compieie report,  entitled  "Interim Protocol for Measuring  Microbial
       Transformation Rate  Constants for Suspended Bacterial Populations in
       Aquatic Systems," (Order No. PB 88-165 7091 AS; Cost: $12.95,  subject
       to change) will be available only from:
          National Technical Information Service
          5285 Port Royal Road
          Springfield, VA 22161
          Telephone:  703-487-4650
  The EPA Project Officer can be contacted at:
          Environmental Research Laboratory
          U.S. Environmental Protection Agency
          Athens, GA 30613
United States
Environmental Protection
Agency
Center for Environmental Research
Information
Cincinnati OH 45268
Official Business
Penalty for Private Use $300

EPA/600/S3-88/007
           rr«;Ufe«o.. ««*
            CHICAGO

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