United States
Environmental Protection
Agency
Municipal Environmental Research
Laboratory
Cincinnati OH 45268
Research and Development
EPA-600/S2-81-231  Jan. 1982
Project  Summary
 Barrel  and  Drum
 Reconditioning
 Industry  Assessment

 C. J. Touhill and Stephen C. James
  An industry assessment was made
of drum reconditioning process char-
acteristics and the current status of
pollutant generation and  disposal.
Typical industry practice for washing
and burning processes for recondi-
tioning  are described along with
operating and design criteria  for
individual unit operations. Processing
procedures that  influence product
quality and environmental pollutant
generation are discussed.  Pollutant
loadings  are defined in   terms of
sources and pathways, major pollutant
parameters, and generation and dis-
position modes.  Current  status of
pollution control practice is defined in
terms of processes and equipment,
operating procedures, disposal prac-
tices, removal efficiencies, and costs.
  This Project Summary was devel-
oped by EPA's Municipal Environ-
mental Research Laboratory, Cincin-
nati, OH, to announce key findings of
the research project that is fully
documented in a separate report of the
same title (see Project Report ordering
information at back).

Introduction
  For many people, the spent 208-L(55-
gal) steel drum has become the symbol
of toxic and hazardous wastes. Even
though drum reconditioning is intended
to support environmentally desirable
goals of recycle, reuse, and safe disposal
of used drums, popular equating of
drums and hazards focuses adverse
attention upon the industry. The U.S.
Environmental Protection Agency (EPA)
recognizes the useful service performed
by reconditioners, but also is alert to
potential problems the industry  may
encounter in meeting high standards of
environmental quality. Because of this
awareness,  EPA  contracted for  the
following information:
  • to  define representative practice
    for barrel and drum reconditioning
    by washing and burning.
  • to  determine the environmental
    impact of reconditioning processes.
  • to  recommend procedures  for
    designing, optimizing,  and retro-
    fitting reconditioning facilities to
    meet rigorous environmental
    standards.
  • to determine the capabilities of the
    reconditioning industry to process
    pesticide and toxic chemical con-
    tainers safely.
  The project is being conducted in
three parts. In the first, current status of
the industry is evaluated in terms of
state-of-the-art practices for both
reconditioning and pollution control. In
the second part, three reconditioning
sites were selected for sampling and
analysis to define more closely pollutant
sources and pathways. The final phase
is the development of recommendations
for design modifications, process
optimization, and  retrofitting recondi-
tioning processes.
  Five sources  of information were
used to prepare the first-phase report:
publicly available literature, transcripts
of National Barrel and Drum Association

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 (NABADA) forums on reconditioning
 problems and techniques, proceedings
 of  four  International  Conferences on
 Steel Drums, responses to a question-
 aire sent by NABADA to its membership,
 and visits to  11  drum  reconditioning
 plants.

 Industry Overview
   During 1979,  about  250 recondi-
 tioners processed more than 41 million
 steel drums. More than 95% were 208-
 L (55-gal) drums;  most of the rest were
 114-L (30 gal). About two-thirds of the
 drums are reconditioned at washing
 plants processing  tight head drums. The
 remainder, open  head  drums, are
 burned in drum reclamation furnaces.
 Facilities that only wash drums account
 for 39% of reconditioning plants;  18%
 only burn; 43% do both.
   NABADA members represent only
 48% of the reconditioning plants in the
 country, but  they process more than
 90% of all washed drums and more than
 97% of those burned. For non-NABADA
 reconditioning facilities, 70% recondition
• for  service and resale, and 30% are
 users who process  only their own
 drums. More  than half  (52%) of the
 drums washed are on  a service of
 laundry  basis; 45% are for resale. By
 comparison, only about one-third of the
 drums burned are on a service basis;
 62% are resold.
   For  many years, the annual  ratio of
 new drums produced to  reconditioned
 has been nearly 1 to 1. Additionally, the
 ratio of new tight to open head drums (4
 to 1) has not changed over the past 10 to
 12 years. Trends, however, show an
 increase in  drum thickness.  For
 example, in 1969, 18-gage or  heavier
 drums comprised 64.3% of those
 manufactured that year. In March 1980,
 that percentage had fallen to 41.4. This
 reduces the pool of potentially recon-
 ditionable drums because thinner
 drums are less able to withstand the
 rigors of transportation  and recondi-
 tioning processes.
   The prime users of new drums are the
 oil and  petroleum  and the industrial
 chemical industries. For  reconditioned
 drums, these two  industries and the
 paint industry are the main users. A
 high percentage  of oil and petroleum
 drums are used and recycled. Because a
 low percentage of chemical drums are
 reused,  it is not surprising that drums
 containing spent industrial chemicals or
 chemical residuals comprise a signif-
 icant number of drums found at aban-
 doned hazardous  waste disposal sites.
Reconditioning Processes
  Steel drums are processed by washing
or burning. Because tight head drums
almost always are washed, recondi-
tioners frequently refer  to washing
facilities  as tight head plants. Con-
versely, open head drums are processed
almost exclusively by burning; hence
burning operations often are called
open head plants.

Washing Process
  Most drum washing is done with
strong hot caustic solution.  Despite
common use of this technique, no tight
head  reconditioning  plants are the
same. Certainly there are many simi-
larities, but for  maintenance  or en-
hancement of environmental  quality
standards, each plant must be evaluated
separately.
  In a washing  plant, the following
operations generally are employed.
After screening and draining upon
receipt, drums are preflushed  using a
strong hot caustic  solution.  Subse-
quently, they proceed to a submerged
caustic washing tank. When drum
contents are difficult to remove using
caustic alone, chains are put  into the
drum along with caustic, and the drum
is tumbled to dislodge adhering mate-
rials. If drum  contents cannot  be
removed by chaining or are cleaned only
with great difficulty, the drum heads are
cut off, thus converting them  to open
heads, and they are sent  to a  burning
plant.  About one-third  of washing
plants remove rust using  hydrochloric
acid washes. Tight head drums then are
rinsed, dedented, shot blasted, leak
tested, and painted.


Burning  Process
  At most burning plants, drums are
inspected upon receipt, and those
containing residues  beyond plant cri-
terion for  emptiness and those con-
taining unacceptable materials are
returned to the shipper along with
damaged drums. Some reconditioners
drain the drums before burning to
reduce temperature excursions due to
materials in the drum. Others believe
that the  best  way to get rid  of the
residuals in the drum is to burn them
directly.
  Some furnaces have water sprays or
steam injection at the inlet opening to
prevent flashbacks and possible operator
injury. Others have built-in distance
barriers to reduce operator exposure to
flashbacks.
  Conveyor belts move drums through
the furnace at an average rate of from 6
to 8 per minute. Average residence time
is 6.6 min. Mean furnace temperature is
675°C (1250°F). All drum reclamation
furnaces use afterburners to control air
emissions. Afterburners are on all the
time at more than .80% of burning
plants. Afterburners operate 95% of the
time considering  an  average of all
plants.  Average temperature  and resi-
dence time for afterburners  is 810°C
(1490°F) and 0.5 sec.  The state  of
California  requires reconditioners who
burn pesticide drums to operate after-
burners at 900°C (1650°F) using a 0.5
sec. residence time.
  When drums  exit the  furnace, they
are either air-cooled  or are water
quenched. About 40% of burning plants
have the capability to quench, but not all
use it all the time. Some only operate
the water quencher when smoky drums
are being  burned or when there is a
visible emission from the drum outlet
opening.  After cooling, open head
drums are shot blasted, dedented, leak
tested,  lined, and painted.
  Natural gas is the preferred furnace
fuel. Where  it  is  unavailable or un-
economical. No. 2 oil is recommended.

Operating Procedures            (
  Most reconditioners have established
procedures for drum receiving and
storage, and nearly two-thirds have  oil
recovery systems.  At a  typical plant,
about 22,700 L (6,000 gal) of oil are
recovered  monthly.
  About  5.4%  of drums bound  for
reconditioning eventually are discarded.
The bulk of these are sold for scrap.
  Almost all  reconditioners  refuse  to
accept drums containing certain mate-
rials. Pesticides are refused by 83% of
reconditioners. Other drums frequently
refused are those formerly containing
ink and those containing adhesives. The
industry processes over 200,000 used
pesticide  drums  per year,  although
there is some uncertainty in this figure.
Most are burned, but a few  plants  do
wash significant numbers of pesticide
drums. Even though the industry claims
that few  facilities accept pesticide
drums, most plants have such drums
scattered within their inventories.
  Plants that process pesticide drums
on a regular basis use special handling
and  processing procedures.  Reported
results  indicate that  burning (using
afterburners at  900°C or  1650°F)
effectively detoxifies  most  pesticide
drums. Additionally, in washing plants,^

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phosphorus and  nitrogen-containing
pesticides lend themselves to detoxi-
fication by alkaline hydrolysis.

Pollutant Loadings
  The  project emphasized  liquid  and
solid wastes in  terms of pollutant
sources and pathways.  Previous  in-
vestigations indicated that air emissions
presented little problem in drum recon-
ditioning.
  Most washing facilities either recycle
and  reuse caustic and rinse waters or
discharge effluents into public sewerage
systems. Nearly 20% of washing plants
claim to have completely closed cycle or
"zero discharge" systems. About half of
all plants  (including those that burn),
claim  to discharge some water  into
public sewers. Only  10% are direct
dischargers after treatment. Mean flow
for a typical facility is 56,800 L/day
(15,000 gal/day).  Because such a high
percentage  of plants discharge to
sewers, water  quality limitations  for
such discharges become very important.
Reconditioning  wastewater is charac-
terized by  high pH, COD, BOO,  and
solids values. There is wide variability in
wastewaters depending upon the types
of drums processed.  There  is some
evidence of hazardous organics in small
concentrations in  some reconditioning
wastewater.
  The  biggest problem  facing recon-
ditioners is  the need  to provide  safe,
economical, and  environmentally  ac-
ceptable means for residuals  manage-
ment.  Evolving solid  and  hazardous
waste management regulations  are
expected to have major effect on  the
industry.  Landfilling  has  been  and
continues to be the predominant method
for residue disposal. Use of incineration
is increasing and  will continue to at an
accelerated rate as the impact of RCRA
regulations are felt.
  On the  average, drums received by
reconditioners contain 2.5 L (0.65 gal)
or 2.5 kg (5.4 Ib) of residues. Caustic
sludges have high pH, COD, BOD, and
oil and grease washing solutions, but in
far greater amounts.
  Preseritly,  surface runoff at recon-
ditioning facilities is not being handled
to any extent.


Pollution Control Practice
and Costs
  Major potential alternatives for  air
pollution control at drum reclamation
furnaces are: (1) direct combustion in
Jhe 650°C (1200°F) to 900°C (1650°F)
temperature range with an afterburner
residence time of 0.3  to 0.7 sec.; (2)
catalytic oxidation in the 315°C (600 °F)
to 510°C (950°F) range; (3) sorption
using activated  carbon, silica gel, or
other  materials; and (4)  scrubber
systems. Worldwide, the direct com-
bustion and afterburner method is the
one most frequently used. Other meth-
ods usually are adjuncts to this primary
method.
  All U.S. reconditioning drum furnaces
have afterburners to consume particu-
lates and organics not burned  in the
furnace main  chamber. About 37% of
drum burning facilities use air pollution
control  equipment and techniques in
addition to afterburners. Typically,
equipment includes scrubbers, packed
towers, baghouses, and dust collectors.
Some methods used to optimize existing
equipment are automatic  ducts to
regulate air flow, and entry and exit air
curtains for better and more efficient
combustion.
  For washing plants, about 55% have
or have under construction their own
wastewater treatment plants.  Water
pollution control equipment being used
includes caustic filters, vacuum  drying
systems, oil/water separators, screens
for gross particle removal, dissolved air
flotation units, flocculation/sedimenta-
tion units,  coalescing plate separators
for oil removal, oil skimmers  (often the
endless belt or rope type), and packaged
wastewater treatment systems.
  Many reconditioners fabricate their
own  pollution  control  systems  as
opposed to using commercially available
products. Operating procedures such as
preflushing, stream segregation, and
cascading  water  use  are important
adjuncts to pollution control equipment.
  The 1980 price for reconditioned tight
and open head drums is about $12.00;
the cost for pollution controls associated
with their cleaning is about  $0.38 for
washing and $0.35 for  burning.


Environmental Assessment
  The  three facilities selected for
testing were: (1) a large drum washing
plant that recycles most of its caustic
washing and  rinsing solutions; (2) a
large burning and washing plant that is
representative  of typical practice;  and
(3) a large washing plant that handles
substantial volumes of pesticide con-
tainers.
  Generally, results of the sampling and
analysis program confirmed typical
ranges of pollutants found in previous
evaluations  of  the  industry. Two ex-
ceptions were:

  (1) Higher concentrations of organic
     compounds, particularly  priority
     pollutants, were evident in aque-
     ous waste streams.
  (2) Lower metals concentrations, for
     most elements, were found in
     aqueous waste streams.
  Based upon  regulatory standards,
results of the sampling and analysis test
program indicated the following probable
methods of pollutant control for the
principal waste  streams of concern:
    (1)  incinerator particulate emis-
       sions - operational controls
    (2)  incinerator organic emissions -
       operational controls
    (3)  incinerator metals emissions -
       operational controls
       and/or bag house filters
    (4)  caustic  washing solutions -
       treatment and reuse
    (5)  rinse  water  - treatment  and
       reuse
    (6)  quench  water - treatment and
       reuse or mixing with other liquid
       streams
    (7)  stormwater runoff - housekeep-
       ing, drainage  control, treatment
       and direct discharge
    (8)  leak tester water - discharge to
       public sewers
    (9)  incinerator ash -  landfill  (con-
       ventional or secured)
  (10)  caustic sludge - treatment and
       either incineration  or  landfill
       (conventional  or secured)
  (11)  drum drainage - treatment and
       either incineration  or  landfill
       (conventional  or secured)


Pollution Control Needs and
Optimization Methods
  It was determined that implementation
of regulations promulgated in conjunc-
tion with  the Resource Conservation
and Recovery Act (RCRA) could have a
positive impact upon drum recondi-
tioners  under the following circum-
stances: (1)  if .the industry  refuses to
accept  drums that formerly contained
materials  listed by  name in 40 CFR
261.33  (e) that have not been triple
rinsed by an appropriate solvent (2)  if
the industry refuses to accept drums
containing residues of hazardous wastes
(other than 261.33  (e)  materials) in
quantities greater than 1 inch; and (3) if
reconditioners avoid  storing accumu-
lated sludge or containers of hazardous
wastes for more than 90 days, and if this

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    sludge  or containers are  not burned,
    buried,  or treated at the reconditioning
    site.
      The following identifies specific areas
    for upgrading and optimizing pollution
    control  at drum reconditioning plants:
      • Operational and management pro-
        cedures
        - receiving
        - storage
        - draining
        - waste stream  segregation
        - water conservation
        - housekeeping
        - waste heat utililzation
      • Pesticide container processing
        - drums  triple-rinsed  before ac-
         ceptance
        - storage in separate area
        - compliance with specified safety
         procedures
      • Air emissions
        - operation  in  accordance with
         NABADA guidelines
        - minimum operational tempera-
         ture of 1200°F
        - minimum residencetimeofAsec
        - afterburner  temperature  of
          1400°F with 0.5 sec residence
         time
        - special operating conditions for
         pesticide drums
        - use of baghouse to control trace
         metal emissions
      • Liquid waste streams
        - segregate all liquid waste streams
        - treated rinse  water should be
          used to make up losses in caustic
         solutions
        - source of quench water  should
         be treated  rinse water
        - management of stormwater run-
         off
            - proper drum storage to include
              berms and dikes for stormwater
              runoff collection
            - proper sludge handling
          • Solid residues
            - testing to determine if solids are
              hazardous
            - operation  control to reduce
              sludge volume
            - proper sludge disposal
            - proper handling of incinerator
              ash
            - processing of recovered oil
            - treatment of hazardous waste
              drum drainage

        Research and Development
          Research and development needs
        identified as a result of this program are:
          (1)  Evaluate whether  incinerator
              particulates, trace metal,  and
              organic emissions- can  be con-
              trolled effectively using opera-
              tional procedures, e.g.,  rigorous
              temperature control, elevated
   temperatures,  variable conveyor
   speeds, drum spacing, and drum
   mixing.
(2) Develop better filtration systems
   for preparing caustic washing
   solutions for reuse.
(3) Determine the feasibility of ultra-
   filtration for  use in processing
   rinse water for reuse.
(4) Develop a strategy for cascading
   water uses (from higher to lower
   quality needs).
(5) Evaluate the potential of good
   housekeeping  and drum storage
   yard management procedures for
   minimizing contamination of
   stormwater runoff.
(6) Develop better processes for
   caustic and rinse water sludge
   dewatering.
(7) Evaluate procedures for disposing
   of non-hazardous sludges and
   residues, including oily waste
   recovery, and sludge burning and
   drying methods.
           C. J. Touhill is with Touhill, Shuckrow and Associates. Inc., Pittsburgh. PA
             15237; and the EPA author Stephen C. James (also the EPA Project Officer.
             see below) is with the Municipal Environmental Research Laboratory, Cin-
           cinnati. OH 45268.
           This Project Summary covers two reports, entitled:
             "Barrel and Drum Reconditioning Industry Status Profile," (Order No. PB
             82-113 382; Cost: $15.00)
             "Drum Reconditioning Process Optimization," (Order No. PB 82-113 374;
             Cost: $9.00)
           The above reports are available only from: (prices subject to change)
                  National Technical Information Service
                  5285 Port Royal Road
                  Springfield, VA 22161
                   Telephone: 703-487-4650
           The EPA Project Officer can be contacted at:
                  Municipal Environmental Research Laboratory
                  U.S. Environmental Protection Agency
                  Cincinnati,  OH 45268
United States
Environmental Protection
Agency
Center for Environmental Research
Information
Cincinnati OH 45268
             Postage and
             Fees Paid
             Environmental
             Protection
             Agency
             EPA 335
Official Business
Penalty for Private Use $300

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