United States
                  Environmental Protection
                  Agency        	
Robert S. Kerr Environmental
Research Laboratory
Ada, OK 74820
                  Research and Development
EPA/600/S2-90/018 July 1990
4>EPA         Project Summary
                   Mobility and  Degradation of
                   Residues at  Hazardous Waste
                   Land  Treatment  Sites at Closure

                   Raymond C. Loehr, David C. Erickson, Laura A Rogers, and Daniel M. Kelmar
                   The objectives of this study were to
                  determine: (a) the  extent to which
                  organics remaining  at  hazardous
                  waste land treatment (HWLT) sites at
                  closure continue to degrade, (b) the
                  migration  potential  of   the
                  accumulated  waste  residue
                  constituents, and  (c) whether
                  available models (RITZ and MINTED)
                  are appropriate for closure decisions.
                  This was achieved  by: (a) obtaining
                  representative soil samples from the
                  treatment zone of several HWLT sites,
                  (b)  characterizing  the  residual
                  material in such samples,  (c)
                  conducting laboratory  studies to
                  determine  the  degradation  and
                  potential mobility of the  constituents
                  in the samples, and (d) using  RITZ
                  and MINTED to evaluate the migration
                  potential of the residual  constituents
                  under different closure options. Soils
                  used were obtained from three sites
                  to  which listed  refinery or wood
                  preserving wastes had been applied
                  and from a site which  had  soil
                  contaminated with coal tar.
                     In the surface soils of the HWLT
                  sites, the concentrations of the
                  organics and metals were greater
                  than in background soils. At depths
                  below 24-30" at the HWLT sites, the
                  concentrations of PAH  compounds
                  were below  detection limits and the
                  freon-extractable  concentrations
                  were   at   background  soil
                  concentrations or  below  detection
                  limits. At sites for which site soil
                  concentrations could be  compared to
                  concentrations in background  soils,
                  the concentrations of chromium and
                  nickel in  site soils  at depths below
24"  appeared  greater  than
background soil  concentrations,
whereas  the  concentrations  of
copper, lead and zinc in site soils at
such depths appeared comparable to
those in background soils.
  Analyses  for organics  in TCLP
extracts of the soils indicated that no
PAH compounds were extracted  by
this procedure from either weathered
or non-weathered soils. Zinc was
found  above detection limits in the
TCLP extracts of the site soils most
frequently. In most of the  site soil
samples analyzed, the concentrations
of metals in the TCLP  extracts were
close to or below detection limits of
0.1 mg/L.
  The PAH and metal concentrations
measured  in the TCLP extracts from
the site soils provided no reason to
conclude that these soils and
accumulated residues  would  fail  to
pass  a toxicity characteristic
determination using the TCLP test.
  The  aerobic  and  anaerobic
microcosm  studies demonstrated
that  there  was  no  statistically
significant degradation of  the PAH
and freon extractables in the zone of
incorporation (ZOI) samples over  an
eight-month period. The data suggest
slow degradation of the accumulated
organics following closure  of  an
HWLT site.
  MINTED is a  predictive model that
estimates  aqueous  equilibrium
solubility concentrations for metals.
However, gaps  in  the  MINTED
database do not allow it to identify
the relative solubility of many of the
metals  of interest at HWLT sites.

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Thus,  MINTEQ appears  of limited
value    for   identifying    the
environmental fate  of metals  under
different closure options.
  When used with worst-case data for
a petroleum refinery  HWLT site, the
modified RITZ  model indicated major
differences  in  mobility  and
persistence of  PAH  compounds
between  capped  and  uncapped
closure  scenarios.  The  closure
options  in  which  the  sites were
uncapped allowed for more  rapid
degradation, but movement  of the
constituents  below  the  ZOI was
greater. For the clay or synthetic cap
option, the degradation of the organic
constituents was much  slower, but
the  movement  below  the  ZOI
diminished. This simulation  indicated
that  the  modified  RITZ model can be
a useful tool for assessing the impact
of different closure  options  on
accumulated residuals at HWLT sites.
  This   Project   Summary  was
developed by  EPA's Robert S. Kerr
Environmental Research Laboratory,
Ada, OK, to announce key findings of
the  research  project that is fully
documented in a separate  report of
the  same  title (see  Project  Report
ordering information at back).

Introduction
  Land treatment has been used to treat
municipal  wastes  for centuries. In
addition, over the past thirty years there
has been increased use  of land treatment
to treat industrial wastes, such  as  wastes
from  the petroleum refining industry. With
the passage of the 1984 Hazardous Solid
Wastes  Amendments  (HSWA)  to the
Resource Conservation and Recovery Act
(RCRA), many changes  have occurred in
the regulatory framework with  regard to
the  use of land-based  technologies for
disposal of hazardous wastes. Due to the
restrictions imposed by these regulations,
a number  of hazardous waste land
treatment (HWLT) sites  are, or soon will
be, undergoing closure. The organic and
inorganic waste constituents that have
accumulated at these sites  can be  of
concern due  to: (a) potential  mobility
during the post-closure period, which can
be  as  long as 30  years, and  (b) the
human and environmental exposure that
might occur when the site is used after
the post-closure period.
  There are several  major options (Table
1) for the closure of  a land treatment site
or a site with  contaminated soils, all  of
which involve the careful management of
the site over the post-closure period,  as
defined  by  the regulations. Both direct
and  indirect  impacts on  human  health
and the environment are important in the
selection of the site-specific  appropriate
closure options.
  The  purpose of  this study  was  to
develop information  pertaining to: (a) the
characteristics  of the waste constituents
remaining at sites having long-term waste
application, such as  HWLT sites, and (b)
the potential for subsequent degradation
and/or  migration of  the constituents  at
such sites.  Such  information  can help
regulatory agencies and industry identify
the most environmentally  sound closure
and post-closure conditions for a specific
site  and can  help  identify  additional
research needs related to the closure  of
HWLT sites.
  Soil samples from  four field sites were
obtained for project  use. The sites were
chosen based  on the following criteria: (a)
waste had been applied at the site for an
extended period of  time, preferably  at
least 10 years, or the waste treatment  or
disposal site had been closed  (unused)
for  an extended period of time, (b) site
history and background information were
available,  (c)  the applied  waste was
representative  of listed refinery wastes
(K-048  to K-052) or  of  listed  wood-
preserving wastes (K-001), and (d) the
site  was available  and accessible  for
sampling. Four sites that most closely
met the  criteria were  chosen.
  The soils evaluated were obtained froi
two operating  HWLT  sites, one  close
land treatment site and a site  which h«
soil contaminated with coal tar. The soi
were  obtained from: (a) the Conoci
Ponca City, Oklahoma, closed  oil refinei
research land  treatment site,  (b)  th
Texaco, Anacortes,  Washington,  HWL
site which  had been in operation sine
1958;  (c) an  HWLT  facility at a woo
treating site (WTS) in Montana; and (d)
Niagara  Mohawk  Power Corporatio
(NMPC) site in New York. The  NMPC sit
was not an HWLT site  and  the  result
from samples obtained at this site shoul
not be  construed to represent  condition
at a managed  HWLT site.
  Two  types  of samples were obtaine
from the Texaco and  the Conoco site:
(a)  surface zone of incorporation (ZO
samples for  a study  to evaluate  th
spatial  distribution  of  residu
characteristics  at such sites and  (b) so
core samples taken  as a function c
depth  to determine whether the  waste
which  had  been applied  to the  surfac
soils had migrated. Only core sample
were taken from  the other   two sites
Although different materials have bee
applied at these sites, similar constituent
were in the  site soils - metals,  long-chai
hydrocarbons,  and  polynuclear aromati
hydrocarbons  (PAH).

Site Soil-Residue
Characteristics
  Results from the  Texaco site indicatee
that volatile  and acid  extractabl<
compounds were not found in  the HWL"
soils but that  PAH  compounds wen
detected  in concentrations considerably
above background. The soils from all fou
sites were evaluated for sixteen specifii
PAH compounds in  the  laboratory
studies.
  The  Texaco site  had  detectable
concentrations of  most of the 16  PAr
compounds in  the top (0-6" and  12-24"
soils   of   the site.  The  average
concentrations of  these compound:
                 Table 1. Options for the Closure of an HWLT Site
                     Removal of the contaminated soil and subsequent disposal of such soil as a hazardous waste.

                     Placement of an impermeable cap over the site. The cap may consist of synthetic liners or clay.

                     The site is left alone with the only continued management being ground-water monitoring as well as run-
                     on and runoff control and a vegetative cover.

                     Continued managed in-situ treatment of the accumulated waste residues.

                     A combination of two or more of the above.

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found  at  increasing depths  from  the
 urrent surface of the site are presented
in  Table 2. The long-term  application of
wastes and residues at this  site  has
raised the topographic surface of the soil
18-42 inches. At the plots sampled, the
surface was increased about 30 inches.
The   absence   of   detectable
concentrations of PAH compounds  in the
36-54" layer  indicated  that  these
compounds had  not  migrated to  this
depth.
  Freon extractable determinations also
were done for the  Anacortes  samples.
This analysis is a relative measure  of the
total oil and grease (0/G) residuals in a
sample. The 0/G concentration in the 0-
6" samples was  61,700  mg/kg and was
56,600 mg/kg in  the 6-12"  sample. The
0/G concentrations in soil samples taken
below 24" were:  24"-36"  --  less  than
1000 mg/kg; 36"-54" ~ 1680 mg/kg;  and
54"-72" -- less than 1000 mg/kg. These
concentrations below 24" were about the
same  as  those in  the  site background
soils.
  The  concentrations of  PAH at  the
Conoco site were  similar  in type  but
much  lower in concentration than  those
found  at  the  Anacortes  site. There  has
been no application of wastes at this site
since 1978.
  The  PAH  concentrations in the  soil
cores  from the plot receiving the largest
application at this site were 'determined.
Below the ZOI, the PAH concentrations
were  close  to  or  below  analytical
detection  limits.  The data indicate that
there has  been no  migration of the PAH
from the surface soils to lower soils.
  The  wood-treating site  soils  had
detectable concentrations of all 16  PAH
compounds except  acenaphthalene and
acenaphthene in  the top layer (0-6") of
the soil.   The concentrations of   PAH
below  the 0-6"  layer  were  very  low,
indicating  that  little or no migration  had
occurred below this depth.

Sample Variability Studies
  Separate surface  soil  samples  were
taken from the Anacortes  and the Conoco
sites  to  determine the  variability  in
characteristics that may  exist in  the
surface soils at a HWLT site. Knowledge
of   this variability  is  important to
monitoring  decisions,  to  closure
conditions and to an  understanding of
whether the core samples  taken from a
site were  representative  of  the
characteristics  throughout the site. The
ZOI samples  were  analyzed for organic
matter, dry weight,  freon  extractables,
ind three  metals  (copper, chromium and
iron).  These  parameters  represent
compounds that  are part of  soil  and of
the  wastes  that  were applied  and
accumulated  in the surface  soils.  The
data from these analyses were compared
using  standard  statistical tests  to
determine whether there was a difference
in chemical  characteristics between  the
sampling locations.
  The  statistical  analyses indicated that
within  the Texaco  and Conoco plots,
consistent differences  in  constituent
concentrations at  each site were  not
observed.  The analyses also indicated
that the residues  that existed  at the time
of sampling  appeared to be uniformly
distributed at the site.
  Based upon a comparison of core and
surface soil samples at the Conoco and
Texaco sites, it appeared that the core
samples were representative  of the soils
at these sites.

Mobility and Weathering
Studies
  These laboratory  studies identified  the
migration potential of constituents in  the
site  soils.  The  effects of  simulated
weathering cycles  on  the  quality  of
potential leachate were determined using
the  toxicity  characteristic leaching
procedure (TCLP). The primary variables
were: (a) soil  samples from  six depth
intervals at  each site,  starting  at  the
surface and proceeding to six feet below
the soil surface; (b) two  weathering
patterns,    Freeze/Thaw    and
Wetting/Drying cycles, and (c) analyses
of TCLP extracts from both  weathered
and non-weathered samples of soil.
  The  methods used  for the simulated
weathering cycles  were adapted from
ASTM  methods for tests of  soil-cement
mixtures. These  procedures  were used
with the soil samples in their  as-received
state, without the addition of cement.
  During  the gas  chromatographic
analysis of  the  approximately  220
extracts analyzed  for  organics, eight
samples had  some measurable  peaks
that could be quantified.  These samples
were analyzed on a mass  spectrometer
and the peaks  identified by a  library
search  of available chemicals.  The results
indicated that  six  of the samples
contained   phthalates,  a   common
laboratory  contaminant,  probably from
plastic  containers  used  during  the
methylene chloride  extraction  procedure.
The two remaining samples  had peaks
which  were   identified  as   long-chain
hydrocarbon compounds.
  The  TCLP  extract  concentrations  for
metals  in soils at the Conoco site as a
function of depth were  as indicated  in
Table 3. These  are  illustrative  of  the
results obtained when the soils from the
other  sites were evaluated. The pattern
was one of low concentrations, generally
about 0.1  mg/L, in the extract from the
surface soils and below detection limits in
extracts from the deeper soils. The one
exception  was  zinc,  which  in some
extracts was above a concentration of 1.0
mg/L.
  The results of these  laboratory studies
can be summarized as follows:
a)Analyses  for organics in the TCLP
  extracts  indicated   that  no  PAH
  compounds were extracted by  this
  procedure from either the weathered or
  non-weathered soils.
b)There  was  no  difference in  the
  concentration of  metals  in  the TCLP
  extract of the non-weathered and the
  weathered samples.
c)The  PAH and  metal  concentrations
  measured in  the TCLP extracts  from
  the  soil/residues from  these four  sites
  provided  no  reason  to conclude that
  the  soils and accumulated  residues
  would  fail  to   pass   a  toxicity
  characteristic determination using  the
  TCLP test  and analysis  of the TCLP
  extract.

Degradation Studies
  These  laboratory   studies were
undertaken to identify the extent to which
organics remaining at closure of a HWLT
or similar  site will  continue  to degrade
under  closure  and  post-closure
conditions. An impermeable  cap will
reduce infiltration and  leaching but also
will restrict oxygen  transfer  from  the
atmosphere.  Anoxic  or   anaerobic
conditions under this type of cover  could
occur.
  Because  of the  expected   soil
conditions with these  closure options,
degradation  under  both aerobic  and
anaerobic  conditions was evaluated and
microcosm  studies were  conducted  over
an eight-month  period.  Only samples
from the Anacortes ZOI were used. Such
samples represent  the  accumulation  of
residues  over 30  years.  The  term
degradation is used  to describe the
results, because it was expected  that
microbial degradation would be the major
organic compound loss  mechanism.
However, the  actual  loss  mechanisms
were not investigated.
  Three separate composites of  four
different  Texaco ZOI  samples  were
prepared  for two  aerobic  and  one
anaerobic  degradation  microcosm
studies. No  uncontaminated  soil  was
added to these samples.  The two aerobic
studies were:  (a) the ZOI  soils without
amendments  or enhancements, and (b)

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       Table 2. PAH Concentrations" at the Texaco Site as a Function of Depth

                                                             Sample Depth"
0-6"
Compound
naphthalene
acenaphthalene
acenaphthene
fluorene
phenanthrene
anthracene
fluoranthene
pyrene
benzo(a)anthracene
chrysene
benzo(b)fluoranthene
benzo(k)fluoranthene
benzo(a)pyrene
dibenzo(a,h)anthracene
benzo(g,h,i)perylene
indeno(i,2,3-c,d)pyrene
Ave.
1.8
BDL
BDL
6.8
5.9
BDL
30
21
BDL
100
130
BDL
204
340
82
38
Range
1-2


4-9
5-8

26-38
16-29

48-155
50-195

47-350
104-600
25-160
14-85
12-24"
Ave.
2.8
BDL
BDL
9.5
25
4.9
75
300
BDL
116
155
BDL
106
194
51
24
Range
2-5
_

6-12
3-39
2-6
19-100
37-432

60-146
31-220

62-136
47-300
8-85
6-40
24-36"
Ave.
1.5
BDL
BDL
0.7
6.7
BDL
BDL
BDL
7.9
4.2
BDL
BDL
1.5
4.1
BDL
BDL
Range
< 1-2.6


< 0.2-2
1-14



< 0.1 -20
2-9


<0.1-3
0.2-10


36-54" Detection
Ave.
2.0
BDL
BDL
BDL
1.4
BDL
BDL
4.0
BDL
0.9
BDL
BDL
BDL
0.8
BDL
BDL
Range Limit +
1.9-2.1 1.0
_ 2.0
_ 1.0
_ 0.2
<0.1-3 0.1
_ 0.1
_ 0.2
<0.1-7 0.1
_ 0.1
<0.1-2 0.1
_ 0.2
_ 0.1
_ 0.1
< 0.2-2 0.2
_ 0.2
0.1
       *   mg/kg dry weight of soil; average of three samples
       BDL below detection limits
       ""   samples from the 6" to 12" depth were not analyzed
        *   detection limit of the analytical procedures used
                Table 3. Average Metal Concentrations * in the TCLP Extracts from the Conoco, 10% Plot Site - Non-
                Weathered Samples
                    Depth      Cadmium    Chromium     Copper        Lead        Nickel         Zinc
0-6" <0.
6-12" <0.
12-24" <0.
24-36" <0
36-54" <0
54-72" <0.
1 0-2 0.1 <03 .1 <0.1
U <0.7
                  mg/L in extract; detection limit was 0.1 mg/L
the ZOI soils with additional nitrogen and
phosphorus. The nutrients were added to
determine  whether  the  addition  of
nutrients to  HWLT  soils  would increase
the loss of organics in these soils.
  The results of  these  degradation
studies indicated  that  there was no
statistically  significant  degradation  of
PAH  and  freon extractables  in the ZOI
soils from the Texaco site over an eight-
month period. It was  in these soils that
the residues from  the  applied wastes
accumulated. The data suggest that there
will be very  slow  degradation  of  the
accumulated organics at  closed  HWLT
sites.
Predictive Models for Closure
  This modeling  effort  was  conducted
simultaneously  with   the  sample
characterization, spatial  variability,
weathering and degradation studies that
were  part  of  the project.  Ideally, the
evaluation  and  use  of  the  predictive
models  should have  occurred after data
were available from the various laboratory
studies.  Such data could have been used
with the  models for a  more focused
evaluation of the models and more direct
comparison of site data to model results.
  This could not  be  done in this  project
because: (a) the  respective models had
to be evaluated  and modified for use
under  closure  and   post-closure
conditions, since the models originall
had not been developed for that purposi
(b)  the modified models  had  to  b
checked to assure that results reasonab!
for  closure conditions  were  bein
obtained, and (c) some  of the laboratot
results, particularly from the degradatic
studies, were not available until very lal
in the project.
  Thus, the input  parameters  to  th
models used in  this  evaluation were m
those  determined  in  the  laborator
portion of this project.  Rather, the  inpi
parameters  and  site-specific  scenario
used were those that were reasonable f<
petroleum refining and  wood  preservin
wastes and for the land treatment  of sue

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wastes.  The values for such parameters
were obtained  from  peer reviewed
literature and from studies in which land
treatment had been used  for  similar
wastes.
  The Regulatory Investigative Treatment
Zone (RITZ) model was used to evaluate
the persistence and  mobility of  specific
organic  constituents. The  MINTEQ model
was used to evaluate the persistence and
mobility of metals. The initial version  of
RITZ was obtained from the Robert  S.
Kerr Environmental Research Laboratory
(RSKERL), U.S.  EPA, Ada, Oklahoma
74820, and the initial version of  MINTEQ
was  obtained from the Center for Water
Quality  Modeling,  Environmental
Research Laboratory,  U.S. EPA,  Athens,
Georgia 30613.
  The RITZ model was modified to:  (a)
function with no waste input,  (b) consider
variations  in  degradation  rate  as  a
function of time, soil depth  and  aerobic
and anaerobic conditions, (c) include the
existence of a  separate oil phase and the
separate degradation  of  the oil phase,
and (d)  utilize  different chemical partition
coefficients  in the  ZOI and LTZ.  The
modified model  was then  used  to
evaluate its use under conditions  likely to
occur at HWLT and  contaminated soil
sites.   The sensitivity of MINTEQ was
examined for  the  three most  important
parameters  that  are influenced  by the
closure  option, pH, the partial pressure of
carbon dioxide gas, and the redox state.
  The  modified  versions  of RITZ and
MINTEQ were used to evaluate  HWLT
closure  options.    The modified  models
were applied to conditions at the Texaco,
Anacortes refinery waste  land  treatment
site.  Considerable data for this site were
available to understand and  evaluate the
applicability  of the models and to model
potential migration of constituents of the
accumulated  residues.   In  addition,
conditions typical of other regions of the
country  also were investigated.
  When  used  with worst-case  Texaco
Anacortes  HWLT site data  at three
different   hypothetical  locations, the
modified   RITZ  indicated   major
differences  between  the capped  and
uncapped scenarios.  The closure options
in which the sites were uncapped allowed
for aerobic conditions, but the movement
of  the  constituents  into  the LTZ  was
greater.   For  the clay or synthetic cap
option,  reduced conditions should occur
and  the movement  into  the LTZ  was
greatly  diminished, due to  the  lack  of
infiltration created by the cap.
  At  the uncapped site, the  persistence,
'.e., potential residence times, of organics
was  estimated to  be approximately 20
years for  benzo(a)anthracene,  and 1100
days for chrysene and  pyrene.  For  the
capped site, 8 of the  12 PAH compounds
examined  remained in the site for 1100
days or more, and 6 of the 12 remained
in the  site for  15  years  or  more.  The
sensitivity of the modified RITZ model to
the differences between  the  various
uncapped closure  options was minimal,
since the bulk of  the  degradation took
place in the ZOI, and the depth constant
did  not  alter these  results.   These
differences are portrayed in Table 4.
  The  results obtained  on  the mobility
and persistence of organics at a HWLT
site under closure  scenarios  indicated
that the modified RITZ can  be a useful
tool for assessing the impact of different
closure options on the migration potential
and persistence of residual organics at
such sites.
  MINTEQ is  able to estimate aqueous
equilibrium solubility concentrations  for
metals  but  is  unable  to estimate  the
actual  mobility  of metals.  Gaps in  the
MINTEQ  database do  not  allow it  to
identify the relative solubility of many of
the metals of interest at HWLT sites. This
evaluation indicated  that  MINTEQ  is
useful  to demonstrate the  potential
mobility of metals as indicated  by  the
relative solubility of metal species and to
determine those most likely to migrate.
  The  results obtained  as  part  of  the
project  provided  insight  into  the
environmental effect of  various  closure
options.   The  most appropriate  option
appears to be one in which the  site is  left
open to the atmosphere. The option of
continued  treatment is beneficial because
the degradation rate  of the  organics  will
be  most  rapid,  and   because  the
conditions used during the active site  life
to prevent metal  migration  will  be
continued.
  This was illustrated when  the  Texaco
Anacortes site  was modeled.   For  the
organics,  no  leaching was predicted  for
the uncapped site,  and  for  the  metals,
there was  no significant increase in metal
solubility under oxidizing conditions. The
results for the capped site indicated that
the residual organics persisted  for a long
time.
  Two important results  were generated
from this  evaluation. One  is that  the
potential persistence  and mobility of  the
accumulated residue constituents  are
affected by  the closure  option chosen.
Another is that RITZ  and  MINTEQ, when
modified to represent closure conditions,
can estimate the potential  mobility and
persistence of  metals and  organics  for
different closure options.  The  actual
choice of a closure option will depend on
such estimates as well as on operational
factors and regulatory concerns.

Conclusions
  The major conclusions from this project
were:
1.  Polynuclear Aromatic Hydrocarbons
    (PAH), freon extractables, and metals
    were  determined  in  the site soil
    samples.   Except for  the coal tar
    disposal  site,  these  chemicals
    accumulated in the  surface  soils.
    The  difference  in  the  coal tar site
    data  is due to the  fact that the
    applied residues  were placed  in  a
    trench rather than being incorporated
    in surface  soils.
2.  In  the surface  soils of  the HWLT
    sites,  the  concentration of the
    organics and metals were greater
    than  in background soils.  At depths
    below 24-30" at the HWLT sites, the
    concentrations of  PAH  compounds
    were  below detection limits and the
    freon extractable concentrations were
    at  background soil concentrations  or
    below  detection limits.   At the sites
    for which  soil concentrations  could
    be compared to  concentrations  in
    background soils, the concentrations
    of  chromium and  nickel in site soils
    at  depths  below  24"  appeared
    greater  than  background  soil
    concentrations,  whereas  the
    concentrations of copper, lead and
    zinc  in site  soils at  such  depths
    appeared  comparable to those  in
    background soils.
3.  A  statistical analysis  of sample
    variability was conducted  using
    surface soils collected at the two
    land treatment sites.  There were no
    consistent  differences in chemical
    concentrations of the surface  soils.
    The analysis also indicated that the
    residues that existed at the time  of
    sampling  appeared to  be uniformly
    distributed  in the  surface soils  of
    each site.
4.  Analyses   for organics  in  TCLP
    extracts of site soils indicated that no
    PAH  compounds  were extracted by
    this procedure from either weathered
    or  non-weathered soils.
5.  There  was no  difference  in the
    concentration of metals in the  TCLP
    extract of the weathered and the non-
    weathered soil samples.
6.  Zinc  was  found  above  detection
    limits  in the TCLP extracts of the site
    soils  most frequently. In most of the
    site  soil  samples  analyzed, the
    concentrations of other metals  in the
    TCLP extracts were close to or below
    detection limits of 0.1  mg/L.

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Table 4. Estimated Persistence and Mobility of Organics Present at the Texaco, Anacortes Site as
Influenced by the Closure Option
^ 	 Leave-Alone Clay/Synthetic Cap
\JiQoiiiC ~ ~ '
Constituent
benzene
ethylbenzene
toluene
o-xylene
m, p-xylene
anthracene
benzo(a)anthracene
chrysene
1 -methylnaphthalene
naphthalene
phenanthrene
pyrene
% Leach
from ZOI
3.7
1.1
3.2
6.6
0.7
0.3
1.4
0.6
0.0
5.4
1.1
10
Time in
ZOI (days)
32
71
55
746
610
720
> 20 years
1100
240
450
720
1100
% Leach
from ZOI
01
0.0
0.0
7.2
0.0
0.0
0 1
0.0
0.0
0.1
01
0.1
Time in
ZOI (days)
100
200
200
> 15 years
720
15 years
> 30 years
30 years
1100
1100
20 years
20 years
7.   The results suggest that the type of
    weathering  used  in this  study
    (freeze/thaw  and  wet/dry) is  not
    expected  to result in an increase in
    organic or metal mobility in soils at
    HWLT sites.
8.   The PAH and  metal  concentrations
    measured in the TCLP extracts from
    the site soils provided no  reason to
    conclude that these soils and
    accumulated  residues  would  fail to
    pass  a  toxicity  characteristic
    determination using the TCLP test.
9.   The   aerobic  and  anaerobic
    microcosm  studies  demonstrated
    that  there  was  no  statistically
    significant degradation of  the PAH
    and freon extractables in  the  ZOI
    samples over an eight-month period.
    The data suggest,  therefore,  that
    there will  be slow degradation of the
    accumulated  organics  at closed
    HWLT sites.
10.  The RITZ  model, as modified  for
    HWLT  site closure  conditions,
    indicated   major differences  in
    mobility and  persistence  of  PAH
    compounds between capped and
    uncapped closure scenarios.  The
    closure  options  in which  the  sites
    were uncapped  allowed  for  more
    rapid degradation, but movement of
    the constituents  below the  ZOI was
    greater.  For  the  clay or synthetic
    cap option,  the  degradation of the
    organic constituents was  much
    slower,  but the movement  below  the
    ZOI diminished.
11.  The  sensitivity  of  MINTEQ was
    examined for parameters  that are
    influenced   by  the closure option:
    pH, the partial pressure  of carbon
    dioxide  and the  redox state.  It was
    difficult  to draw  general  conclusions
    about the effects of these  changes,
    since different  metals  beha\
    differently in solution.   In  gener;
    most  of  the  metals  present
    solution  as  cations  became  le;
    soluble as the pH  increased, and ;
    the partial pressure of carbon dioxk
    increased.  No general statemen
    could  be  made  about  rede
    conditions, as the most soluble red<
    state of  a  given metal varies  fro
    metal to metal.
12.  Based on the low migration potent!
    of   PAH   compounds,  free
    extractables and metals in the  soi
    at  HWLT  sites determined  fro
    laboratory  and model simulatic
    studies, it does not appear necessa
    to cap such  sites at closure. Both tt
    leave-alone  option, or  the option
    continue active site managemer
    appear to  be  protective of hum;
    health and the environment.

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  R. C. Loehr, D. C. Erickson,  L. A. Rogers, and D. M. Kelmar  are  with the
  Environmental and Water Resources Engineering Program, The  University of
  Texas ,  Austin, TX 78712-1076.
  Scott G. Huling is the EPA Project Officer (see below).
  The  complete  report,  entitled  "Mobility  and  Degradation of  Residues at
        Hazardous Waste Land Treatment Sites at Closure," (Order No. PB 90-
        212-564AS; Cost: $23.00, subject to change) will be available only from:
            National Technical Information Service
            5285 Port Royal Road
            Springfield, VA 22161
            Telephone: 703-487-4650
  The EPA Project Officer can be contacted at:
            Robert S. Kerr Environmental Research Laboratory
            U.S. Environmental Protection Agency
            P. O. Box 1198
            Ada, OK 74820
United States
Environmental Protection
Agency
Center for Environmental Research
Information
Cincinnati OH 45268
Official Business
Penalty for Private Use $300
 ICIAL MAIL"
U.S.POSTAGE

SO 35
EPA/600/S2-90/018

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