United States
                    Environmental Protection
                    Agency
Municipal Environmental Research   -
Laboratory
Cincinnati OH 45268
                    Research and Development
EPA-600/S2-83-104  Feb. 1984
&EPA          Project Summary
                   Granular  Activated  Carbon
                   Adsorption and  Fluid-Bed
                   Reactivation  at  Manchester,  New
                   Hampshire

                   David Kittredge, Robert Beaurivage, and David Paris
                     This study was designed to evaluate
                    the actual cost and performance of a
                    fluidized-bed,  granular activated car-
                    bon (GAC) reactivation system, a semi-
                    automatic GAC transport system, and a
                    GAC  water treatment system  at the
                    Manchester Water Works, Manchester,
                    New Hampshire.
                     GAC performance was monitored in
                    one of the utility's four 38,000-m3/day
                    (10-mgd) GAC filters to obtain an initial
                    performance  comparison of  virgin
                    carbon  and reactivated 5-year-old
                    service carbon. This filter was divided at
                    its midpoint and then  operated and
                    monitored until a steady-state condition
                    was achieved in  both filter  media
                    studied. Two  additional reactivation
                    runs were  conducted on this same
                    GAC, providing performance data over
                    three  full  reactivation-exhaustion cy-
                    cles. For a portion of the study, the GAC
                    filter medium  was educted through  a
                    semiautomatic transport system retro-
                    fitted  to the existing filters. Operation
                    of this semiautomatic system proved to
                    be unreliable, however, and was subse-
                    quently abandoned and replaced by  a
                    handheld eductor system. GAC from
                    the three remaining plant filters was
                    also reactivated to obtain additional
                    performance data and to restore the
                    adsorptive capacity of the spent service
                    carbon.
                     Treatment performances of the virgin
                    and reactivated GAC were evaluated
                    during each cycle by  measuring total
                    organic carbon (TOC), trihalomethanes
                    (THM), and trihalomethane formation
                    potential (THMFP). GAC adsorptive
capacity was also measured using
traditional test parameters including
iodine number, molasses decolorizing
index, Brunauer-Emmett-Teller (BET),
and pore-size distribution analyses.
  With the cooperation of three regional
water utilities, a short-term program of
regional reactivation was also investi-
gated. The actual costs and feasibility
of transporting and reactivating GAC
from these utilities were determined.
  This Project Summary was developed
by EPA's Municipal Environmental
Research Laboratory, Cincinnati. OH.
to announce key findings of the research
project that  is fully documented in a
separate report of the same title (see
Project Report ordering information at
back).

Introduction
  In keeping  with the research goals of
the Safe Drinking Water Act (Public Law
93-523), the U.S. Environmental Protec-
tion Agency (EPA) and  the Manchester
Water Works (MWW)  entered into a
cooperative agreement  to evaluate the
cost and performance of a fluidized-bed,
GAC reactivation system plus related
facilities at the  Manchester Water
Treatment Plant. GAC effectiveness was
assessed before and after reactivation,
and GAC reactivation for other water
utilities in New England was calculated
on a limited basis. All of the work
associated with this project was done
under actual  operating conditions using
full-scale water treatment equipment.
  On completion of the water treatment
plant in 1974, MWW officials began

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investigating alternatives for reactivation
or replacement of approximately 432,592
kg  (500 tons) of  GAC used  at the
151,000-mVday (40-mgd) water treat-
ment facility. Results of this investigation
demonstrated that  onsite reactivation
was the most cost-effective method of
restoring the adsorptive properties of
spent GAC  for the conditions studied.
  Water treatment at Manchester consists
of flash mixing followed by flocculation,
sedimentation,  and  series  filtration
through individual beds of sand and GAC
filter media Raw water is obtained from a
naturally occurring,  highly protected
surface supply (Lake Mussabesic), which
contains no volatile organics but occasion-
ally has high color plus taste and odor as a
result of algae formation
  Since the research  project spanned a
period of nearly 5 years (July 1977 to
April  1982), the investigation  was
divided into three major phases. Phase 1
involved the  design,  construction, and
startup  of the fluid-bed reactivation
system (see  Figure 1), semiautomatic
carbon transport system, and laboratory
monitoring  facilities. One of the four GAC
filters  in the  treatment plant called "the
test filter"  was half  filled with  virgin
carbon and half with reactivated service
carbon to  compare GAC filter media.
After about 90 days, exhausted GAC (as
    Spent GAC
determined  by  TOC and  THMFP) was
removed from the filter, reactivated, and
then reintroduced to the filter for another
90-day period of service and performance
evaluation.
  Phase 2 involved two more cycles of
reactivation and repeated evaluation of
the test filter. The three other GAC filters
in the treatment plant were reactivated a
total  of five times to  determine  the
operational  performance capabilities of
the reactivator and to develop reactivation
cost data. Losses from both reactivation
and transport of GAC were also studied.
  After all the objectives of the first two
phases were achieved,  the third  phase
was undertaken to study the possibility of
using the Manchester treatment facility
as  a regional reactivation center. The
major  objective of this program was to
establish  the economic  feasibility of
providing a future GAC reactivation
service for other water utilities in the New
England region. Approximately 18,144kg
(40,000 Ib) of GAC  from  each of three
separate  utilities was reactivated and
subsequently returned to service  during
1982.

Significant Findings
  The Manchester research project
demonstrated that onsite GAC reactiva-
tion at a medium-sized water treatment
                                    Westvaco
                                    Fluid Bed
                                   Reactivator
                                                               Recycle Gas
                                                                 Blower
                                          Steam Generator
             Eductor

Figure 1.    Process flow for GAC reactivation system at Manchester, New Hampshire.

                                    2
facility is feasible with regard to cost and
operation. A fluid-bed reactivation furnace
was shown to be a practical addition to a
water treatment operation, provided that
a properly trained, full-time work force is
available to operate and  maintain the
equipment. During the 10 months from
June 1980 to March 1981, more than 1.8
million Ib of GAC was reactivated at a
total cost of less than 22
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Table 1.    Manchester Water Works Reactivation Costs. June 1980 Through March 198V
Cost Item
Makeup carbon
Labor for reactivation
Labor for transportation
Labor for laboratory
Labor for administration
Parts and service calls
Fuel oil
Electrical power
Water
Laboratory supplies and outside
analyses
Depreciation
Overhead
Cost/kg
1C)
15.59
4.28
0.62
0.11
291
5.87
4.92
1.10
1.63

0.11
4.70
6.08
Cost/lb
1C)
707
1.94
0.28
0.05
1.32
2.67
2.23
0.50
0.74

0.05
2.13
2.76
                        TOTAL
47.92
21.74
*Based on reactivation of 842,401 kg (1,857,176 Ib) of GAC.
tion, poor reliability, excessive  mainte-
nance, and unacceptable removal of filter
media. A  manually operated hose and
eductor system was then substituted and
used successfully to transport GAC
between  the  filters  and reactivation
building.
  Because of the success of the research
program,  the  Manchester facility was
investigated for  use  as  a regional
reactivation  center. This final research
effort demonstrated  that  MWW  could
economically provide a GAC reactivation
service for other water utilities in the New
England region.  The combined  average
reactivation cost  was 49.5C/lb.
  The  full report was  submitted  in
fulfillment of Cooperative Agreement No.
CR805371 by the Manchester Water
Works under the sponsorship of the U.S.
Environmental Protection Agency.
   David Kittredge, Rober Beaurivage. and David Paris are with the Manchester
     Water Works, Manchester, NH 03103.
   Ben W. Lykins. Jr., is the EPA Project Officer (see below).
   The complete report, entitled "Granular Activated Carbon Adsorption and Flu id-
     Bed Reactivation at Manchester, New Hampshire. "(Order No. PB 84-110238;
     Cost: $25.00, subject to change) will be available only from:
          National Technical Information Service
          5285 Port Royal Road
          Springfield, VA 22161
           Telephone: 703-487-4650
   The EPA Project Officer can be contacted at:
          Municipal Environmental Research Laboratory
          U.S. Environmental Protection Agency
          Cincinnati, OH 45268
                                                   GOVERNMENT PRINTING OFFICE 1984-759-015/7299

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