United States
                    Environmental Protection
                    Agency
Industrial Environmental
Research Laboratory
Research Triangle Park IMC 2771
                    Research and Development
EPA-600/S7-84-080 Sept. 1984
&ERA          Project Summary
                    Evaluation  of  Natural-  and
                    Forced-Draft Staging Air  Systems
                    for  Nitric Oxide  Reduction   in
                    Refinery  Process  Heaters
                    R. C. Benson
                     Results of pilot-scale tests to evaluate
                    combustion modifications for emission
                    reduction and efficiency enhancement
                    on  petroleum process heaters are re-
                    ported. Objectives were to determine
                    nitric oxide (NO) emission reductions,
                    thermal efficiency changes, long-term
                    performance, and cost of both natural-
                    and forced-draft staged-combustion-
                    air  modifications. Forced-draft staged-
                    combustion-air modifications had been
                    shown to be the  most promising
                    combustion modification  in previous
                    pilot-scale tests. The test unit was  a
                    vertical, cylindrical, natural-draft crude
                    heater, and the test fuels were natural
                    gas, refinery gas, and a combination of
                    No. 6 oil and refinery gas. The unit had a
                    16  MW heat input capacity and was
                    capable of a  maximum throughput of
                    108 mVh of crude oil (rated input 96
                    mVh).
                     A natural-draft staging  air system,
                    capable of providing 50 percent of the
                    staging air for 100 percent refinery gas
                    firing and crude charge rates of 55 - 90
                    percent rated capacity, reduced NO
                    emissions  by about 50 percent. The
                    stack Oa was lowered from 4 percent
                    baseline to 2 percent low NO condition.
                    The efficiency gain  with the natural-
                    draft staging air system was about 1.5
                    percent. Natural-draft staged combus-
                    tion air (4 percent stack  O2) with 80
                    percent oil/20 percent gas  firing
                    provided NO reduction of 30 percent
                    and an average efficiency  gain of 0.6
                    percent.  Lowered  excess air  with
                    staging (4 to 2 percent Oz) for the
                    80/20 mix provided an NO reduction of
about 60  percent and  an average
efficiency  gain of 3.6 percent,  but
unacceptable CO emissions and smok-
ing problems. While firing 80 percent
oil/20 percent gas, the forced-draft
staging air system provided about 40
percent of the total combustion air and
an  NO reduction of 40 percent  (6
percent baseline stack Oa to 3 percent
low NO stack O2). The efficiency gain
with the forced-draft staging air system
was 5 percent. A 15-day evaluation of
the natural-draft staged air system
revealed  no special operating difficul-
ties or process constraints. Costs of the
natural-  and forced-draft staged air
systems are compared. The natural-
draft system (staging with lowered
excess air)  has a cost of $0.03/lb NO
on  29.3 MW  natural-draft process
heater, compared to $0.32/lb NO for a
forced-draft system.
  This Project Summary was developed
by  EPA's  Industrial Environmental
Research Laboratory, Research Triangle
Park, NC, to announce key findings of
the research project that is fully docu-
mented in a separate report of the same
title (see Project Report ordering infor-
mation at back).


Introduction
  The test work reported here includes
results of combustion modifications for
NO control on a refinery process heater.
The crude heater tested is the same one
described in EPA Contract 68-02-2645.
The heater  is a natural-draft, vertical,
cylindrical  crude heater containing six

-------
burners, capable of gas and/or oil fuel
firing. Of the advanced combustion
modification concepts considered for NO
control, staged air lances were considered
a feasible approach. The test program has
two objectives with respect to staged air
lances: (1)  to  evaluate the potential of
natural-draft staged air lances for reduc-
ing NO emissions and increasing thermal
efficiency;  and (2) to  evaluate  the
performance of a staged air system on a
heater firing 100 percent residual oil. The
heater could not be run on 100 percent oil
as originally hoped. The original plan was
to have a temperature controlled valve in
the oil line to automatically adjust oil and
gas flow rates to  satisfy thermal  input
requirements.  Since the valve was  never
installed, the crude oil outlet temperature
was automatically controlled  by gas flow
and manually  controlled by oil flow. For
safety and control, the plant could not run
the heater solely on manual control. The
staged air system has 24 ports (4 per
burner) through which either  natural-
or forced-draft staged air may pass.
  Table 1 summarizes the  significant
results obtained during  the  pilot-scale
test program.  Natural-draft staged com-
bustion air  lowered NO  emissions by
about 45 percent,  while  low excess air
decreased NO emissions by  20 percent
with 100 percent gas firing. The stack O2
was maintained at about 4 percent for the
staged air test and lowered from 4 to 2
percent for the low excess air test.  In a
short  term test,  the  combination of
natural-draft staged combustion air and
lowered excess air reduced NO emissions
by about 50 percent (4.1 to 2.6 percent
stack Oa) while decreasing gas consump-
tion about 1 -2 percent.
   Forced-draft staged combustion air
with 80 percent oil/20 percent gas firing
(6 percent  stack O2) lowered NO  emis-
sions by about the same amount (20-25
percent) as low excess air with no staging
(6 to 4 percent 02). Lowered excess air
together with  staged combustion air
reduced NO emissions by 40 percent (6 to
3  percent 02) on  natural-draft vertical
cylindrical heater firing 80 percent oil/20
percent gas.
  In addition to the testing described,  a
15-day  evaluation of the natural-draft
staged  air  system  was made.  Cost
analyses of the natural- and forced-draft
staged air systems were  performed to
compare the two systems.

Test Heater Description
  The test unit is a natural-draft, vertical,
cylindrical crude oil process heater, used
to supply a heated charge to a crude oil
distillation column. A maximum load of
108 mVh (16,250 bbl/d) could be sent
through the heater in two passes. The
rated capacity of the heater is 91.8 m3/h
(14,000 bbl/day).
  The maximum firing rate of the heater
is  16.1  MW thermal input (55 x  106
Btu/hr). It is fired by six John Zink DBA-
22 natural-draft burners. The burners are
combination gas/oil burners rated at  a
maximum of 2.68 MW(9.14x 106Btu/hr)
each  with a  turndown  ratio of 3:1.
Although combination gas/oil  burners
are used, some  gas is  always fired
because the unit is base loaded on oil fuel
and an automatic temperature controller
adjusts the gas fuel flow to maintain crude
oil outlet temperature.

Staged Air Systems
  The forced draft system consisted of 24
vertical 316L stainless steel pipes of 3.18
cm (1-1/4 in.) diameter arranged four-
per-burner, 90  deg.  apart. A 45-deg.
elbow on  each  pipe provided better
mixing across the flame. A fan supplied
air to the lances through a manifold and
flexible tubing. The lances could be varied
in height up to 1.2m (4 ft) from the floor of
the  heater. Extensions for  the  lances
allowed staging heights up to 2.4 m (8 ft)
for oil firing tests.
  For the natural-draft system, holes
were drilled through the heater floor so
that  one end of the 4-in. pipe would be
flush against the heater floor and the
other end (threaded for pipe caps) would
protrude a few  inches below the heater
floor. For the  natural-draft staged air
tests, the pipe caps were removed and 1 -
1/4  in.  lances,  3-in. lances,  or the 4-in.
ports were used.


Emissions Test
Instrumentation
  All emission measurement instruments
(see Table 2) were carried in a 12.8 x 2.4
m (42 x 8 ft) mobile laboratory trailer. The
Table 2.    Emission Measurement Instrumentation
Species
Carbon Monoxide
Oxygen
Carbon Dioxide
Nitrogen Oxides
Particulates
Sulfur Dioxide
Particle Sizing
Smoke Spot
Opacity
Sulfur Oxides
Manufacturer
Beckman Instuments
Teledyne
Beckman Instruments
Thermo Electron Co.
Andersen Samplers. Inc.
DuPont Instruments
Andersen Samplers, Inc.
Bacharach


Measurement Method
IR Spectrometer
Polarographic
IR Spectrometer
Chemiluminescent
EPA Method 5 Train
UV Spectrometer
Cascade Impactor
ASTM 21 56-65
EPA Method 9
Goksoyr-Ross
Model
No.
865
326A
864
10A
EPA
400
Mark III
RCC


Table 1.    Summary of Combustion Modification Tests on a Pilot-Scale Process Heater
Heat
Input
/WM/T
14.2
12.8
12.9
15.6
14.4
10.7
9.4
13.6
15.2

Fuel
fief.
Ref.
Ref.
Ref.
Ref.
80%
80%
80%
80%

Gas
Gas
Gas
Gas
Gas
Oil/20%
Oil/20%
Oil/20%
Oil/20%






Gas
Gas
Gas
Gas

Baseline
Oz.%
4
4.2
3.6
4
4.1
3.8
4.1
5.7
6.1

Combus.
Mod.
Oz.%
3.9
3.8
3.4
2.0
2.6
3.8
2.0
4.1
3

Baseline NO
ng/J
67
73
70
78
78
135
167
140
176

ppm dry
at 3% Oz
131
142
138
152
152
265
328
344
345

Percent NO Reduction
Staging from Baseline
Air %
40
33
8
b
45
41
__b
b
39

43
21
12
21
46
25
28
13
37

Change in Fuel
Consumption, % Combustion Modification3
-1.1
0
+1.8
-1.3
-1.4
-4.5
-2.4
-2.5
-6.0

ND (SCAj 4" ports
ND fSCAJ 3" lances
ND fSCA) 1-1/4" lances
LEA
ND ISCA + LEA) 4" ports
FD (SCA)
LEA (4% + 2% Oz)
LEA (5.7% + 4.1% Oz)
FD (SCA + LEA)
6% + 3% O2
aFD = forced draft, LEA - lowered excess air, ND = natural draft, and SCA = staged combustion air.
b/V0 staging.

-------
 gaseous species measurements were
 made with analyzers located in the trailer.

 Baseline Conditions
  Baseline conditions were  4 percent
 stack Oa for 100 percent gas firing and 4 -
 6 percent stack Os for 80 percent oil/20
 percent gas firing. The 4 percent stack 02
 for 100 percent gas firing is considered to
 be  a normal  operating  level by plant
 personnel.  The 4 percent stack 02
 baseline for 80 percent oil/20 percent
 gas firing was also considered to be  a
 viable  starting point by plant pesonnel
 and also would permit direct comparison
 of NO emission data previously collected
 at the 50 percent oil/50 percent gas firing
 condition (Ref.  EPA-600/7-83-022). Base-
 line stack Oz  of 4 percent was initially
 achieved  for  several test days under
 various thermal input rates and crude
 charge rates. However, some test series
 at  the  low and medium loads from
 February 22, 1983, onward could not be
 run at 4  percent baseline Oz without
 making  extreme stack  damper and
 register adjustments. It is  not clear why
 the 4 percent baseline Oz was more diffi-
 cult to achieve on  some test  days.
 Reasons may include the crude inlet
 temperature change (which alters the fuel
 input to maintain constant crude outlet
 temperature) or the fuel composition ratio
 (80 percent oil/20 percent  gas) which
 was not burning effectively at lower stack
 02  levels. These baseline conditions
 could  be  achieved  solely with  stack
 damper  and  secondary air register
 adjustments (i.e., no combustion modifi-
 cations). The 4 percent stack Oz for 100
 percent gas firing and 6 percent stack 02
 for the 80/20 oil/gas mixture was
 achievable  under all  process  rates
 studied (55-96  percent full load). The
 baseline conditions were established to
 determine the extent of NO reduction to 2
 percent stack Ojon 100 percent gas firing
 and typically 3 percent O2 on an 80/20
 oil/gas mixture.

 Results

 Natural-Draft Staged Air
  Three staged air  injection configura-
 tions were tested using 4-in. ports, 3-in.
 pipe, and 1-1/4 in. pipe, respectively.
 Load was maintained  nominally at 80
 percent rated capacity and stack 02 of  4
 percent  for  testing  with  the three
 configurations. The 4-in.  ports provided
the most staging air: about 40 percent of
the total combustion air.
  The 4-in. ports achieved the greatest NO
 reduction.  A reduction of about 45-50
percent was  achieved from  baseline
conditions (SCA only).
  The burner equivalence ratio,
$B=   (air/fuel)bumer
     (air/fuellstoictuometric

was about  0.72 with the secondary air
registers   10 percent open. At this
minimum  $>&  NO emissions decreased
47 percent below the baseline of 131 ppm
dry at 3 percent 02 (67 ng/J).  The 4-in.
ports are  flush with  the  heater floor;
whereas, the  pipes  could  be inserted
through the ports to introduce the staging
air higher above the heater  floor.
  Since the 4-in. ports  had  provided the
most staging and  NO  reduction of the
diameters tried, further testing with load
variations  and Oz variations were con-
ducted with the 4-in.  ports. The three
loads tested were 55, 80, and 90 percent
                                         rated  capacity with  Oz variation from
                                         about 2 - 6 percent stack Oz. Under these
                                         conditions, the CO concentration levels
                                         measured were  minimal, and flame
                                         impingement was not a problem.
                                           Figure  1 shows the effect of staging
                                         (decreased burner equivalence ratio) on
                                         NO emissions. The crude charge rate for
                                         this test  series was  52.7  rnVhr (8000
                                         bbl/day), 55 percent of rated capacity. For
                                         each Oz  level (2,4 percent), the burner
                                         equivalence  ratio was lowered in incre-
                                         ments by closing the stack damper and
                                         closing down the burner air registers to
                                         50,33, or 10 percent open. The minimum
                                         $B for any 02 level was that associated
                                         with the registers  10  percent open. At 4
                                         percent Oz (SCA only), the minimum 4>e
                                         obtained was 0.63 (48 percent of total air
                                         is staged air) which reduced NO emissions
                                         48 percent below the baseline of  152
   200
   180
   160
   140
   120
$ 100
to
I
E'  80
o'
    60
   40
   20 h
                       1
            Fuels: Absorber Gas
            Process Rate: 13.1 kg/s (8000 bbl/d)
            4" Ports, Natural-Draft Staged Combustion Air
                           (10/25-41

                       (10/25-7R)


                      (10/25-7)

                    (10.25/8) |
                                    I (10/25-5)
            • Baseline.
            ™ no staging
             (all combustion air
             through burners}


             Stack Oa
             approximately 4%
    D2% Oa (Staging + Low Excess Air)
    NO = 11.34 + (124.3 X&B)
    r2 = 0.98

(~\ 4%0z (Staging)
V-X NO = 3.60 + (123.9 x <*>B)
    r2 = 0.97
                               I
             0.2     0.4      0.6      0.8      1.0

                           a. Burner Equivalence Ratio
                                                       1.2
                             1.4
1.6
Figure 1.
           NO emissions at two different stack Oz concentrations as a function of burner
           equivalence ratio.

-------
ppm, dry at 3 percent 02. At 2.3 percent
O2 (SCA + LEA from a stack 02 percent of
3.7), the minimum $B obtained was 0.58
(51  percent of total air is staged air) which
reduced NO emissions 51 percent below
the baseline.
  Percent changes in fuel  consumption
with NO reduction  were calculated to
show  the  extent of fuel savings  with
staged  air combustion modification,
lowered excess air, and staged  air
combined with lowered  excess  air.
Staged combustion air at 4 percent and 2
percent O2 (no lowered excess  air)
showed consistent NO reduction rates 45
- 50 percent. Average fuel savings are on
the order of 0.5 - 1 percent. The fuel
savings become more significant (on the
order  of 1 - 2 percent) with staged air
combined with lowered excess air.

Forced-Draft Staged Air
System
  Tests were initially conducted with the
forced-draft  staged-combustion-air sys-
tem to assess the levels of NO reduction
attainable at various staging heights and
burner equivalence ratios. Only 1-1/4 in.
lances were tested with the forced-draft
system. The optimum stage height for NO
reduction and minimal CO and smoke
was determined to be 4 ft with the lance
tips oriented toward the burner center-
line.
  Figure 2 shows NO emissions  as a
function of burner equivalence ratio for
two O2 levels.  The staging height  for
these tests was 1.2 m (4 ft) and the crude
charge rate was  76 m3/h  (11,500
bbl/day). The $B was decreased in incre-
ments to its minimum value determined
by limitations of the staged air combus-
tion fan. At 4 percent O2, the minimum <|>B
(maximum staging)  obtained was  0.71
which decreased NO emissions 24 per-
cent below the baseline of 265 ppm NO,
dry at 3 percent stack 02. About 40 per-
cent of the total combustion air was injec-
ted through the 24 1-1/4 in. lances for
the 4 percent stack 02 tests, while 29 per-
cent of the total combustion air was in-
jected through the lances for the 6 per-
cent stack 02 tests. The lower percent
staged air for the 6 percent stack O2 tests
is due in part to the higher fuel heat input
rate that day.
  The efficiency gains were significant
with 80 percent oil/20 percent gas firing
and forced-draft staged combustion air.
The change in fuel consumption relative
to baseline when SCA was applied was
3.5 percent for 6 percent stack 02.  Low-
ered excess air and forced-draft staged
combustion air reducesfuel consumption
by 6 percent.
 Natural- Versus Forced-Draft
 Staging
   Figure 3 compares the effectiveness of
 natural-  with forced-draft staged air for
 NO reduction only. In this instance, the
 process  rate was  maintained at about
 14,000 bbl/day and stack O2 maintained
 at 4  percent for baseline  and staging
 conditions. The  results show that, for
 maximum staging (minimum 4>B), the 4-
 in. ports (NDSCA) and 1-1/4 in. lances
 (FDSCA) provide very comparable NO
 reduction for about  the  same  staging.
 Note  that the 1-1/4 in. lances of the
 forced-draft system mixed the air and fuel
 better, resulting in  lower  amounts of
 smoke and CO compared with the  4-in.
 ports of the natural-draft system.
           Long Term Test (Natural-Draft
           Staging with 3-in. Lances)
             Figure 4 shows the baseline and
           staging data  of  NO  versus stack Oz.
           Linear regression analyses were run for
           both the baseline  and  staged-air data
           points. The linear  regression analysis
           shows a very good correlation  for the
           staged air data (coefficient of determina-
           tion, r2  = 0.9), while the coefficient of
           determination is  fairly good for the
           baseline  data (r2 = 0.78).  Calculations
           with the linear curve fit equations were
           performed to determine the extent of NO
           reduction with staging  only (SCA) and
           a combination of staging and low excess
           air (SCE + LEA). The NO reduction from
           baseline is about 15 percent with staging
   500
   450
   400
   350
6§" 300
   250
t
a
  200
   750
   700
   50
           Fuels- 80% #6 Oil, 20% Gas
           Staging Height: 4 ft
           Crude Charge Rate. J 1,500 bbl/day
    (2/17-3J


(2/17-4)
                                                      (2/17-1,5)
                                     v-'     •• 12/14-1
                                                (2/14-1)

                                                (2/14-5)
                                     (2/14-2)
                            (2/14-3,4)
         ^1 ^P Baseline, no staging


         Q 4% 02
            NO = 98.9 + (138.7 x B)
            r* = 0.99

         Q 6%O2
            /VO= 157.5+ (135.8 xB)
                   I
                                             I
                  0.4           0.8            1.2
                          cj>a. Burner Equivalence Ratio
                            1.6
                                                                      2.0
Figure 2.    NO emissions as a function of burner equivalence ratio for two stack Oi
           concentrations.

-------
only, and about 28 percent with staging
and low excess air.

Cost Analysis of Staged
Combustion Air Applied to a
Natural-Draft Process Heater
  Total annualized costs for 16.1, 29.3,
and  147  MW thermal  input process
heaters were calculated for SCA,  LEA,
and SCA + LEA. These total annualized
costs were then divided by the annual
N0< reduction potential (Table 3) to give a
dollar amount per  metric ton of  NOX
removed by the  modification  (Table 4).
The  savings of natural-draft staged
combustion air on a natural-draft process
heater  applied at normal stack 02 are
calculated as $714/Mg NOX  reduction
for  a 16.1  MW heater,  increasing to
$964/Mg at 147 MW heat input.  The
cost of natural-draft staged air  combined
with lowered excess air on a natural-draft
crude heater is calculated as  $336/Mg
NOx  reduction for 16.1  MW unit and  a
savings of $435/Mg NOX reduction for a
147 MW unit. The net cost at lower unit
heat rates with the combined modification
is due  to an automatic stack draft
controller that permits operating the
heater at lowered Oa.
400
350
                                          300
                                          250
                                       B
                                          200
                                        o
                                       O
                                          150
                                          100
                                          50
Fuels: 80% Oil/20% Gas

Crude Charge Rate: 14,000 bbl/day
Stack Oxygen: 4%
                                                                     (2/28-4)
                                                         Baseline, no staging
       LJ Forced Draft Staged Combustion Air
           <1-14" lances)
           NO = 128.3 + (143.2 x <*>„)
           r' = 0.91
                                                     Natural Draft Staged Combustion Air
                                                     (4" ports)
                                                                       I
                                                         0.3           0.6           0.9

                                                                a. Burner Equivalence Ratio
                                                                                                1.2
                                                                                                             1.5
                                        Figure 3.    NO emissions as a function of burner equivalence ratio for natural- and forced-draft
                                                   staged air.

-------
    150
    120
  I
     30
              Crude Charge Rate: 11,500 bbl/day /18.9 kg/s)
              100% Gas Firing
                    I
Baseline (3/31-4/1)
MO = S2.0 + (8.6xO2.%)
r* = 0.79
8 data points (21 hours total)

3" Lances -Staging Air (3/1 6-3/30)
                                        6 data points (113.3 hours total)
                    /
                                                        4
                                      Stack Oz,%, Dry


Figure 4,    NO versus O2 under baseline and staging conditions.

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Table 3.   Annual NO Reduction Potential of Combustion Modifications for Three Heater Sizes
Modification/Test Series
Natural-Draft Staged Combustion Air,
700% Gas Firing (4% QJ / 10/8/82
Natural-Draft Staged Combustion Air
+ Lowered Excess Air, 100% Gas
Firing (4% + 2% Oz) / 10/27/82
Lowered Excess Air, 700% Gas Firing
(4% + 2% Oi) / 10/27/82
Lowered Excess Air, 50% #6 Oil/50% Gas
Firing (4. 1% + 1.8% Oif
Lowered Excess Air, 80% #6 Oil/20% Gas
Firing (4.5% + 1.8% Oz) / 2/1 1/83
Baseline
NO (ng/J)
67
73
67
114
176
ng/J
Reduction
30
40
10
32
60
% Reduction
from Baseline
45
55
IS
28
34
»vu ni
76.7 MW
10.7
14.2
3.7
11.4
18.1

29.3 MW
19.4
25.9
6.8
20.7
33.0

147 MW
97.7
129.7
34.1
103.8
165.4
"Mg/yr = megagrams per year.
"Tidona. R.J. et al., "Refinery Process Heater /V0« Reductions Using Staged Combustion A ir Lances," EPA -600/7-83-022 (NTIS No. PB83-193946).
 March 1983.
Table 4.    Cost Effectiveness Ratio of Combustion Modifications Applied to Three Natural-Draft Process Heater Sizes

                                               161MW                       29.3 MW
                                                                                                          147 MW
   Modification
               Annual  Cost
     Total       Reduc.   Effec.
Annual/zed Costs  Poten.   Ratio
   $ (Savings)    Mg/yr'  S/Mg
               Annual  Cost
     Total       Reduc.   Effec.
Annual/zed Costs  Poten.   Ratio
   S (Savings)    Mg/yr'  S/Mg
               Annual  Cost
     Total       Reduc.  Effect.
Annual/zed Costs  Poten.   Ratio
   $ (Savings)    Mg/yr"  $/Mg
Natural-Draft Staged Combustion Air
10O% Gas Firing (4% Oz/
Natural-Draft Staged Combustion Air
17.642)
4.775
10.7
14.2
(714)
336
(15.593)
1.770
19.4
25.9
(804)
68
(94. 146)
(56.475)
97.7
129.7
(964)
(435)
   Lowered Excess Air. 10O% Gas
  Firing (4% + 2%
Lowered Excess Air, 100% Gas Firing
Firing (4% + 2% Oil
Lowered Excess Air. 8O% #6 Oil/20%
Gas Firing (4.5% + 1.8% OJ
Lowered Excess Air, 50% #6 Oil/50%
Gas Firing (4. 1% + 1.8 % O2
872
(30.516)
(18.914)
3.7
18.1
11.4
218
(1,686)
(1.659)
(3.755)
(60.798)
(39.652)
6.8
33.0
20.7
(543)
(1,842)
(1.911)
(68.263)
(354,201)
(248.270)
34.1
165.4
103.8
(1.997)
(2.141)
(2,392)
'Mg/yr - megagrams per year.
   R. C. Benson is with KVB, Inc., Irvine, CA 92714.
   Robert E. Hall is the EPA Project Officer (see below).
   The complete report, entitled "Evaluation of Natural- and Forced-Draft Staging Air
     Systems for Nitric Oxide Reduction in Refinery Process Heaters," consists of
     two volumes:
       "Volume I.  Technical Report," (Order No. PB 84-229 640; Cost $20.50,
       subject to change).
       "Volume II. Data Supplement," (Order No. PB 84-229  657; Cost  17.50,
       subject to change).
   The above reports will be available only from:
           National Technical Information Service
           5285 Port Royal Road
           Springfield, VA22161
           Telephone: 703-487-4650
   The EPA Project Officer can be contacted at:
           Industrial Environmental Research Laboratory
           U.S.  Environmental Protection Agency
           Research Triangle Park, NC27711
                                                                            . S. GOVERNMENT PRINTING OFFICE: 1984/759-102/10699

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United States
Environmental Protection
Agency
Center for Environmental Research
Information
Cincinnati OH 45268
Official Business
Penalty for Private Use $300





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