vvEPA
                                 United States
                                 Environmental Protection
                                 Agency
                                 Environmental Research
                                 Laboratory
                                 Corvallis OR 97330
                                 Research and Development
                                 EPA-600/S3-81-018 July 1981
Project Summary
                                 Some  Effects of
                                 Petroleum  on  Nearshore
                                 Alaskan  Marine Organisms

                                 D. G. Shaw, L E. Clement, D. J. Mclntosh, and M. S. Stekoll
                                  The overall objective of this project
                                 was to better understand the effects
                                 of chronic, low-level oil pollution on
                                 nearshore Alaskan marine organisms.
                                  The bivalve mollusc Macoma bahhica
                                 accumulated hydrocarbons during
                                 180 days of continuous exposure to
                                 Prudhoe Bay crude oil in flowing
                                 seawater dispersions with nominal
                                 concentrations  of 0.03 mg/l~1, 0.3
                                 mg/r1 and 3.0  mg/l*1. The animal's
                                 ability to concentrate oil from seawater
                                 increased with decreasing oil in water
                                 concentration. Decreases in Mbahhica's
                                 oil burden began after 30 to 120 days
                                 (depending on the oil concentration)
                                 and continued for at least 60 days
                                 after oiling ceased. Alipathic and
                                 aromatic hydrocarbons were fraction-
                                 ated in markedly different ways by the
                                 animal. Branched and cyclic aliphatics
                                 in the range dodecane through hexa-
                                 decane were preferentially retained
                                 over their higher homologs, whereas
                                 larger and more substituted aromatics
                                 were selectively concentrated.
                                  Macoma balthica showed a number
                                 of physical, behavioral, physiological
                                 and biochemical changes during oil
                                 exposure. An oil in seawater concen-
                                 tration of 3.0 mg/r1 caused severe
                                 dysfunction in the clams including a
                                 decreased burial rate, increased respi-
                                 ration rate, and inhibition of growth
                                 leading to very  high mortalities. The
                                 lowest concentration of oil tested,
                                 0.03 mg/r1 will in time lead to popula-
                                 tion decreases.
                                   This Project Summary was devel-
                                 oped by EPA's Environmental Research
                                 Laboratory, Corvallis, OR , to an-
                                 nounce key findings of the research
                                 project that is fully documented in a
                                 separate report of the same title (see
                                 Project Report ordering information at
                                 back).
                                 Introduction
                                   Understanding and predicting the
                                 cumulative impacts of chronic, low level
                                 petroleum discharges are particularly
                                 difficult because the environmental
                                 changes induced are generally gradual
                                 and often extremely difficult to distin-
                                 guish from natural environmental fluc-
                                 tuations. This project was an effort to
                                 improve our scientific understanding of
                                 the fate and effects of long term, low
                                 level petroleum exposure on marine
                                 organisms. This extremely broad topic
                                 was narrowed to a tractable investiga-
                                 tion by setting the following conditions:
                                   • We were  principally concerned
                                     with invertebrate intertidal animals
                                     common to Alaskan and other
                                     northern waters.
                                   • We wish  to focus on sublethal
                                     physiological  and biochemical
                                     changes which might effect the
                                     viability of populations, rather than
                                     on processes of hydrocarbon me-
                                     tabolism.
                                   • We wanted to investigate animals
                                     exposed to environmentally realistic
                                     oil concentrations.

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  • We would monitor the kinds and
    amounts of hydrocarbons to which
    the animals were exposed and
    which they incorporated in order to
    correlate petroleum burdens with
    biological effects.
  After a series of preliminary investi-
gations we determined that the most
promising approach would be to work
with the small deposit feeding clam,
Macoma balthica, under controlled con-
ditions in the laboratory. Although this
species has no common name, it is
circumpolar in distribution and occurs
abundantly in intertidal and shallow
subtidal areas of fine grained sediments
north of about 40° latitude. We felt that
the stresses caused by bringing the
clams into the artificial environment of
the laboratory were offset by our in-
creased ability to manipulate and moni-
tor oil exposure in a controlled setting.
  In order to provide a realistic simula-
tion of chronic exposure of marine
animals to oil-in-seawater dispersions
in the laboratory, we constructed a
continuous-flow system capable of
simultaneously delivering dispersions
with nominal oil in water concentra-
tions of 0.03 mg/r1,0.3 mg/l"1 and 3.0
mg/l"1. Through the course of our
experiments we quantitatively mea-
sured the concentrations of various
aromatic and aliphatic petroleum hydro-
carbons in the clams and the seawater
to which they were exposed. For this we
used the techniques of gas chromato-
graphy and computerized gas chromato-
graphy-mass spectrometry. We exposed
clams for six months to oil and in
seawater dispersions and maintained
another group of clams free of oil but
otherwise under identical conditions in
the laboratory, to serve as controls.
Numerous biological parameters were
monitored during the six month oil
exposure test and for an additional two
months afterwards.
Results
  Figure 1 shows the total hydrocarbon
burden of oil exposed and control clams
during and for two months after the
experiment. These data reveal two
important facts:

  • Clams exposed to each oil concen-
    tration began to reduce their body
    burden of petroleum before the end
    of exposure.
  • Although the "high exposure"
    clams were  in water containing
70,0001-
 7,000 -
f
•*w
1
1
•9
I
   100
                                       Figure 1.
                                          "72CT
                                Days of Exposure
            Macoma balthica tissue concentrations of total hydrocarbons during
             180 days of exposure to oil in seawater dispersions and 60 days of
            recovery. Bars show the range of duplicate determinations; dots are
            single determinations.
     100 times as much oil as the "low
     exposure" clams, after six months
     oil exposure, the body burdens of
     clams from the two exposure levels
     differed by only about a factor of
     four.
  Chemical analysis showed that not all
of the constituents of petroleum were
taken up or retained by the clams to the
same extent. For the aliphatic hydro
carbons we  found,  as have  other;
previously,  retention by the animals is
greatest for ring compounds, less foi
branched compounds, and  least fo
straight chains. We also found tha
within the cyclic and branched aliphatic

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 Hydrocarbon series, lighter molecules
were retained more strongly than their
heavier cogeners. Aromatic hydrocarbons
as a group were taken up in preference
to aliphatics but for these compounds
heavier  homologs were selectively
accumulated.
  Table 1 gives a summary of the bio-
logical condition of clams exposed to oil
for six months as compared to unexposed
controls. Clearly the animals subjected
to the two higher oil in water concentra-
tions, 0.3 mg/r1 and 3.0 mg/l"1, were
adversely affected in numerous ways;
feeding decreased, mortality increased,
weight and growth decreased, gonads
appeared abnormal and enzyme activities
were altered. Clams exposed to 0.03
mg/l"1 oil were in most ways not signifi-
cantly different from controls. However,
in two critical respects these  clams
differed from the control group. These
exposed clams grew only 20% as much
as the controls. This difference is highly
significant according to standard statis-
tical  tests.  In addition microscopic
examination  of these exposed clams'
gonads showed that reproductive mate-
           rials were being resorbed rather than
           brought to maturity for spawning. It
           seems clear that conditions which
           impair functions as basic as growth and
           reproduction threaten the viability of a
           population.
             This work suggests  that sublethal
           exposure of Macoma balthica to petro-
           leum  results in two distinct groups of
           adverse effects. The first group includes
           several alterations of behavior which
           indicate  that oil exposed clams are
           sluggish and disoriented. These effects
           include decreased burial rate, decreased
           feeding rate and decreased general
           activity. The  onset of these behavioral
           changes occurs within one week of
           initial oiling.  Similar effects have been
           reported in numerous short term acute
           oiling effects studies. The second group
           of adverse effects appears to be related
           to a negative energy balance in the oil
           exposed animals. These effects include
           decreased dry weight,  abnormal and
           resorbed gonads and decreased carbo-
           hydrate content. These effects begin to
           appear only after 60 days of exposure
           and appear not to be simply a conse-
Table 1.    Summary of the Effects of Six Months of Oiled Seawater on Various
           Parameters of Macoma balthica
                                      Level of oil in exposure tanks
  Parameters measured
0.03 mg/l
0.3 mg/l
3.0 mg/l
1. Behavior
general activity
burying rate
% unburied
feeding rate
2. Mortalities
3. Respiration rate
4. Physical
wet weight
dry weight
dry/ 'wet ratio
growth
condition index
5. Morphology
gonads
gills
6. Biochemical
protein
carbohydrate
lipid
DNA
RNA
Mg^-ATPase
Na*-K*-ATPase
5'-nucleotidase
phosphodiesterase

normal*
normal
normal
normal
normal
normal

normal
normal
normal
decreased
increased

reabsorbed


normal
normal
normal
normal
normal
normal
normal
increased?
normal

decreased
decreased
increased
decreased
increased
normal?

normal
decreased
decreased
decreased
decreased

abnormal


normal
decreased
normal
normal
normal
normal
normal
increased?
normal

decreased
decreased
increased
decreased
increased
increased

decreased
decreased
decreased
decreased
decreased

abnormal


normal
decreased
increased?
normal
normal
decreased
normal
increased?
increased
                                    quence of decreased feeding activity.
                                    Bivalves normally offset a decrease in
                                    food intake by decreasing their meta-
                                    bolic rate and thus are able to endure
                                    prolonged periods with little or no food.
                                    However, in the oiled M. ballhica the
                                    decrease in feeding was compounded
                                    by an increase in metabolic activity as
                                    measured by respiration rate. It appears
                                    that these two effects together are
                                    responsible for the negative energy
                                    balance in the oiled clams. Certainly
                                    each of these groups  of effects will
                                    adversely impact Macoma balthica,.
                                    affecting  the  viability of exposed indi-
                                    viduals and populations.


                                    References
                                    Portions of this research have  been
                                    published:
                                      Clement, L.E., M.S. Stekoll, and D.G.
                                      Shaw. Accumulation, fractionation
                                      and release of oil by the intertidal
                                      clam Macoma balthica. Marine Biol-
                                      ogy 57, 41-50 (1980).
                                      Stekoll, M.S., LE. Clement, and D.G.
                                      Shaw. Sublethal effects of chronic oil
                                      exposure on the intertidal clamMacoma
                                      balthica. Marine Biology 57, 51-60
                                      (1980).
^normal, decreased, increased - are levels relative to those in the controls.
                                                                                      
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      D, G. Shaw, L. E. Clement, D. J. Mclntosh, andM. S. Stekollare with the Institute
        of Marine Science, University of Alaska, Fairbanks, AK 99701.
      Barry Reid is the EPA Project Officer fsee below).
      The complete report, entitled "Some Effects of Petroleum on Near shore Alaskan
        Marine Organisms," (Order No. PB 81-159 147; Cost:  $9.50,  subject to
        change) will be available only from:
             National Technical Information Service
             5285 Port Royal Road
             Springfield, VA 22161
             Telephone: 703-487-4650
      The EPA Project Officer can be contacted at:
             Environmental Research Laboratory
             U.S. Environmental Protection Agency
             Corvallis, OR 97330
United States
Environmental Protection
Agency
Center for Environmental Research
Information
Cincinnati OH 45268
Postage and
Fees Paid
Environmental
Protection
Agency
EPA 335
Official Business
Penalty for Private Use $300

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