United States
Environmental Protection
Agency
Environmental Monitoring Systems
Laboratory
Research Triangle Park NC 27711
Research and Development
EPA-600/S4-83-051 Nov. 1983
Project Summary
Technical  Assistance
Document:  Quality Assurance
Guideline  for  Process  Feed
Rate Monitors  in  the Portland
Cement  and  Lime  Industries
Robin R. Segall and John R. Richards
  This study, sponsored by the Quality
Assurance Division of the U.S. Environ-
mental Protection Agency's Environ-
mental Monitoring Systems Laboratory,
evaluated the performance of process
feed rate monitors used in the Portland
cement and lime industries. Particulate
emission regulations applicable to both
industries are specified as kilograms of
particulate per megagram of feed to the
process. Regulatory agencies have
assumed that feed rate  monitors are
highly accurate due to process control
considerations; this study evaluated the
validity of this assumption.
  This study has found that  six major
types of feed rate monitors are currently
used in the Portland cement and lime
industries. Each of these monitor types
is reliable and accurate; seldom do the
errors exceed ±3 percent, and in most
cases the monitor performance allows
control of the process flows to within +1
percent. This performance level is
necessary (1) to ensure that the resulting
products meet specifications, and (2) to
minimize kiln and  calciner  operating
problems. Operating personnel routinely
check the operation of the  feed rate
monitors and calibration  is carried out
frequently.
  In the majority of cases, regulatory
agencies could assume that the process
feed rate monitors are  sufficiently
accurate. However, if some question
should arise concerning the  monitors,
the evaluation procedures listed in this
report may be used to verify  accuracy.
The following material also includes a
summary of typical problems and
calibration techniques associated with
the monitors.

  This Project Summary was developed
by EPA's Environmental Monitoring
Systems Laboratory, Research Triangle
Park, NC, to announce key findings of
the research project that is fully
documented in a separate report of the
same title (see Project Report ordering
information at back).

Introduction
  The New Source Performance Stand-
ards (NSPS) and many State Implementa-
tion Plan (SIP) regulations contain several
emission rate limits specified per process
operating rate, as shown below:
       Pollutant emission rate
       Process operating rate
In the  NSPS, this type of emission
standard is found in Subparts F and HH,
which contain the Standards of Perform-
ance for Portland cement  plants and
lime manufacturing  plants, respec-
tively.1'2 In these two subparts, the
allowable emission limits for particulate
matter are expressed per unit of process
weight, as indicated by the following:

Portland Cement Plants (Subpart F)
 0.15 Kg per metric ton of feed (dry basis)
   to the kiln
Lime Manufacturing (Subpart HH)
 0.15 Kg per megagram of limestone feed
   [to the rotary kiln]
 0.075 Kg per megagram of lime feed [to
   the lime hydrator]

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  In  the  past, a substantial effort has
been directed towards the quality assu-
rance (QA) of the numerator  in these
expressions, while the accuracy of the
denominator remained unquestioned.
For process control  reasons,  agencies
have routinely assumed the denominator
is accurate.
  This report examines the information
available on the accuracy and reliability of
data  from these monitors. In addition to
the current literature, equipment vendors
and  plant operators  were consulted to
obtain information concerning types and
applications of these monitors, reported
accuracy, sources of error, operation and
maintenance procedures, calibration
procedures,  and general evaluation
procedures.  This  report includes an
introductory section that  discusses the
types and typical locations  of process feed
rate monitors for the Portland cement a nd
lime  industries. The operation  and
routine calibration of each of the major
types of  monitors typical of these
industries are described  in section 2.0.
This  section also addresses the quality
assurance  aspects of  each type of
monitor  including  accuracies, typical
errors and problems, preventive mainte-
nance, and visual evaluation techniques.

Operation, Calibration and
Evaluation of Process Feed
Rate Monitors
  This examination  into the use of
process feed rate monitors in the Portland
cement and lime industries revealed that
six main types of monitors are commonly
used. These are:  (1)  the gravimetric
weigh belt  scale, (2)  the gravimetric
weigh belt feeder, (3) the  nuclear weigh
belt scale, (4) the impact  flowmeter, (5)
the pneumatic weigh feeding system, (6)
the plunger-type feeder,  and (7) the
magnetic  flowmeter.  This section will
examine  each of these  major monitor
types.

Gravimetric Weigh Belt Scales
  Gravimetric weigh belt  scales are the
most basic form of gravimetric contin-
uous-weighing devices. The normal
weigh belt scale is part  of a  material-
handling conveyor belt system and
supports a portion of the moving conveyor
belt. It uses a mechanical  lever or load
cells to instantaneously weigh the amount
of material carried on that portion of the
belt. Weigh belt scales are used in both
the lime industry and the Portland cement
industry. When used for kiln monitoring,
weigh belt  scales usually  act as  a
materials balance check,  in conjunction
with another weigh feeding device which
actually provides the consistent kiln feed
rate.

Accuracy
  For factory approved installations,
manufacturers guarantee load cell-type
weigh  belt scales to weigh and totalize
with an error not to exceed 0.5 percent of
full  scale, 3'4 while  mechanical type
scales  may have claimed accuracies of
±0.25  percent or better.5

Calibration
  There are three common methods for
calibration of gravimetric weigh belt
scales. These are: using a  material test,
using test chains, or using test weights. A
fourth  method, electronic calibration, is
not as  commonly seen.6'7
  A  typical calibration scheme involves
use of a material test for initial belt scale
calibration  upon installation8'9 and then
use  of a test weight or test chain
calibration monthly thereafter.9 Evidence
that  an instrument is  performing incor-
rectly, of course, indicates that a calibra-
tion  should be performed immediately.

Evaluation  Checklist
  In  summary, the  following checklist
may be useful as a guide for routi ne visual
examinations of gravimetric weigh belt
scales.
  •  Belt  scale  is being  operated  at
     between 50 and  90 percent of its
     rated capacity.
  •  Belt loading is uniform in flow and
     symmetry.
  •  No material lumps are larger than
     15 percent of belt width.
  •  There is no  material  or  water
     movement in the  belt  scale area.
  •  There is a gravity or tension take-up
     on a belt longer than 40 ft, and it is
     located near the head pulley.
  •  Unloaded belt runs completely in the
     idler trough (at correct belt tension).
  •  Belt scale is located near the bottom
     or tail end of the  conveyor.
  •  Belt  scale is  acceptable distance
     from convex or  concave  curves,
     load-in and load-out  points, skirt-
     boards, and trippers.
  •  Belt conveyor does not  have "V"-
     type idlers, five  roll  deep  trough
     idlers, rope or cable  support rolls
     type idlers, offset carry rolls, or
     center rolls.
  • Scale mounted  idlers and three
     stationary idlers  to either side  are
     dimensionally aligned (within 1/32
     in.).
  • Belt tracks centrally at all load
     conditions.
  • There  are no training idlers within
    six idlers of the scale.
  • Troughing angle of idlers is < 35°.
  • A windbreak is provided if the scale
    area is subjected to >5 mph winds.
  • The ambient temperature in the scale
    area is within the specified operating
    range for that model.
  • There  is no dust  build-up on  the
    weighbridge, belt, or speed sensor.

Gravimetric Weigh Belt
Feeders
  Gravimetric weigh belt feeders  are
somewhat  similar to gravimetric weigh
belt scales in  that they weigh flowing
material with  a scale  applied to  a
conveyor belt. However, the scales weigh
material (usually on its way from one place
to another) without  concern  for  the
amount delivered per unit of time;  the
weigh  belt feeder, on  trie  other  hand,
weighs material (on a short belt) in order
to deliver  a specified amount in  a
specified time and usually at a constant
rate. A weigh belt feeder usually includes
feedback controls to achieve this goal.

Accuracy
  Because  of their shorter belt  lengths,
weigh feeders tend to be more accurate
than comparatively sophisticated weigh
belt scales. The  literature and  vendors
cite accuracies of up to ±0.25 percent10'11
of set rate, and at least ±0.5 percent11 or
±0.5 percent to ±1 percent of set rate.5

Calibration
  Gravimetric weigh belt feeders  are
calibrated in the  same  manner as
gravimetric weigh belt scales; that is, by
using material tests, test chains, and test
weights (see previous section).

Evaluation Checklist
  The following  items  may be  used tc
perform a visual evaluation of a weigh
feeder.
  • Load  is at least 50  percent  ol
    capacity.
  • Belt  is loose  enough to permi'
    deflection at weigh area.
  • Belt has tension roll or some othei
    assurance  that it  does  not slip or
    drive and measurement pulleys.
  • Weigh idler(s) or weighdeck i)
    aligned.*
  • There is little or no dust build-up 01
    weigh deck, platform, etc.
  • There is no dust build-up on pulleys
  • Belt is tracking correctly.
*To check al ignment place a string between the fixe
 or stationary idlers; it should barely touch the weic
 idlers.

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Nuclear Weigh Belt Scales
  Like the gravimetric weigh belt scale
systems, nuclear weigh belt scale systems
are not generally used as direct kiln feed
rate monitors. Instead, they  are usually
part of a larger materials  balance check
system. However,  the nuclear monitor
can  be  used to measure mass flow in
material transfer systems other than a
conveyor  belt.12  It has  been applied
directly  to proportioning screw feeders,
and to the combination system used for
kiln feed rate monitoring and control.13

Accuracy
  Stated accuracy varies between ±0.75
percent and ±1 percent depending upon
application and manufacturer. 3l  4'15
Discussions with plant  operators who
use  these  instruments  have indicated
typical  accuracies  of 1  percent with
source drift occasionally causing errors as
great as 3 percent.9'16

Calibration
  The two principal methods of nuclear
weigh belt scale calibration are the dyna-
mic material test procedure and the static
calibration plate (or material) procedure.
Most nuclear scale manufacturers rec-
ommend conducting a material test for
the  initial  calibration.  Recalibration is
then performed on a monthly basis using
the  calibration  plate that  is usually
supplied with the weigh scale.17

Evaluation Checklist
  The previous discussion suggests  the
following checklist for nuclear weigh belt
scale evaluation.
  • Belt loading is between 70 and 100
     percent of rated capacity (or at least
     greater than 2.7 Ib/ft2).
  • Belt loading does not vary by more
     than 30 percent on a regular basis.
  • Product profile does not appear to
     change significantly.
  • Product does  not include  lumps
     larger than 15 percent of belt width.
  • Scale is not used to weigh more than
     one material or material bulk density
     without recalibration.
  • There is no material slippage in the
     vicinity of the scale.
  • There is no material build-up on the
     detector.
  • There is no material build-up on the
     belt.
  • There is no water running on  the
     belt in the weighing area.


Impact Flowmeters
  This type of process monitor is designed
for  use  as an  in-line  flowmeter  for
measuring solids, liquids, and slurries. In
the Portland cement and lime industries,
it finds typical application in the weight
measurement of solids less  than 3 in. in
diameter. Impact flowmeters make
material flow measurements by sensing
the force produced by the material as it
free falls (by  gravity) onto a  sensing
device. Two types of sensing devices are
currently used in impact flowmeters: the
impaction plate and the impaction cone.
The former device is used in the majority
of installations in the lime  and cement
industries, therefore the following dis-
cussion will focus almost exclusively on
the impaction plate type of flowmeter.

Accuracy
  Impact flowmeters are quite accurate;
manufacturers generally claim 0.5 percent
of full  scale, and comments from plant
instrument operators confirm this.9'18'19

Calibration
  As with the weigh belt scales and  the
nuclear scales  discussed  previously,
initial calibration of an  impaction plate
flowmeter  is usually  accomplished by
using a material test  and  subsequent
recalibration uses a static test "weight."
The  initial material test calibration is
recommended upon installation, with
recalibrations performed  at  monthly
intervals  (more often  if  required by
special circumstances or if warranted by
inconsistent readings).9
  Some of the newer flowmeter system
installations may have a third calibration
check that utilizes a bin-load cell weighing
system.8

Evaluation Checklist
  The  previous  section suggests the
following visual  inspection points to be
used in routine impact flowmeter evalua-
tion.
  •  The material flow  impacts on the
     center of the sensing plate or cone.
  •  Flowmeter  is  used for only  one
     material (unless material change
     calibration  compensation is built
     into the electronics).
  •  There is no appreciable buildup of
     dust'in the impingement area of the
     impaction plate (or cone).
  •  There is no airflow against the plate
     (or cone).  Note:  Most of these
     devices are enclosed so this may not
     be a problem.
  •  Material measured by the flowmeter
     does not change in particle shape or
     hardness.
  •  Plant maintenance procedures  for
     flowmeter include ensuring that it is
     kept properly leveled.
   • The  flowguide  assembly  is  the
     proper one for current material and
     flowrate.


Pneumatic Weigh Feeding
Systems
  Polysius Corporation, a major design/
construction firm for cement plants,
recently  installed pneumatic weigh
feeding systems in five U.S  plants. The
system is marketed  under the name
POLDOS®.20'21'22'23
  Raw meal is fed from the homogenizing
silos through a set of control valves to a
bucket elevator. The meal is dumped into
a calibration tank mounted on load cells,
then metered out of this tank by a control
valve. The meal passes down an airslide
to the pneumatic conveyor, which trans-
ports the material to the  top of  the
preheater. The mass flow from the
pneumatic conveyor is linearly related to
the floor pressure below  the pneumatic
conveyor (AEROPOL®) aeration surface.
The pressure is converted by a transducer
into  an electrical control signal for  the
main solids flow valve located under the
calibration bin. By  using the  pressure
level as an indicator of flow, it is possible
to eliminate the weigh belt feeder which
used to be installed below the calibration
bin.

Accuracy
  Polysius claims an accuracy of better
than 1  percent which is equivalent to the
accuracy claimed for conventional weigh
feeding systems.21

Calibration
  The POLDOS® system is calibrated by
interrupting  the material  flow to the
calibration bin and allowing the raw meal
to empty out for a period of time.22'23 The
difference in  the calibration bin weight
before and after the test is compared with
the pressure value. A number of tests at
different  feeding  rates  are  used  to
generate the complete calibration curve.
Examples of these calibration curves are
available in references 22 and 23. As part
of the  overall  calibration procedure,
the load cells on the calibration bin  are
checked by hanging various weights on the
side of the bin.21

Evaluation
  Polysius reports  no serious problems
with the  operation  of the POLDOS®
system,21 which is entirely enclosed and
has no external mechanical parts which
could be checked. Because of this, agency
observers must rely  strictly on plant
calibration data.

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Plunger Type Feeders
  Lime plants with rotary kilns  and
preheater towers generally use a plunger
type feeding mechanism to del iver the hot
limestone feed to the kiln.24'25'26'27'28 By
controlling the length of the stroke and
the frequency of operation, it is possible
to achieve the desired volumetric feed
rate.24'28 Depending on the design of the
preheater, the system may be equipped
with 4 to 18 of these feeders.24'2*27''*

Calibration
  Calibration of the feeders can be
accomplished in a manner analogous to
that used to calibrate the impaction flow
monitors and the POLDOS® system. The
stone feed bin can be mounted on  load
cells and emptied over a period of time in
order to relate the plunger operation to
the mass of material fed. High-  and low-
level indicators in the stone bin could be
used  in lieu of the load cells. They can
also be calibrated using material balance
checks.

Evaluation
  Since the feeding mechanisms are
mounted  internally  on most  types of
preheaters,  it is impossible for  any
agency observer to  evaluate their  per-
formance. The kiln rotational  rate  may
provide one index of the feed rate since
the feeding system is synchronized with
the kiln speed.
Magnetic Flowmeters
  Because  of their  ability to measure
volumetric flows of abrasive slurries,
magnetic flowmeters find prevalent use
for kiln feed rate monitoring  in the wet
process  cement  industry.  These flow-
meters measure, over a period of time,
the flowrate and total flow of the blended
raw material slurry sent intothe kiln.This
flowrate  can  be converted to dry  raw
material  mass flowrate by taking  into
account slurry density (which remains
reasonably constant). One  plant uses a
magnetic flowmeter in conjunction with a
density meter.29'30 The density meter is
generally a nuclear  density gauge that
measures slurry weight per gallon.

Accuracy
  Magnetic flowmeter accuracy differs
slightly from manufacturer to manufact-
urer but  many claim ±1 percent of full
scale or  better.31  Some manufacturers
claim accuracies of ±1 percent of actual
flow,32 and others go as  low as  ±0.5
percent of full scale.33
Calibration
  Magnetic flowmeter calibration is
almost  always  performed  using an
electrical simulator;32 however, in cases
where maximum accuracy is required, a
comprehensive water  calibration that
uses a calibration rig is essential.34 The
simulator is connected  to the electrode
wires in the transmitter, and simulates
normal conductor fluid voltages through
the flowtube for different flow velocities.32
The transmitter is checked to ensure that
these readings agree with the simulator
readings. Because this type of calibration
requires that the process be shut down,
and  because  magnetic  flowmeters sel-
dom, if ever, drift from calibration, these
flowmeters are usually calibrated only
once, at the time of installation.32

Evaluation Checklist
  A magnetic flow monitor is usually not
subject to serious operational problems.
However, if data confirmation is desirable,
the following  checklist may be of assist-
ance. Since  the  instrument is totally
enclosed, the extent to which  proper
operation can be checked is quite limited.
  • Check the monitor installation to
     confirm  that  the  site is free of
     serious flow disturbances.
  • Confirm that instrument  is properly
     grounded, and grounding is free of
     corrosion,  by  visually checking
     ground strap or area.
  • Compare instrument reading to kiln
     rotational speed.


References
 1.  U.S. Environmental Protection Agency,
    Standards, of Performance for  Port-
    land  Cement  Plants, CFR Part 60,
    page 248767, December 23,  1971.
 2.  U.S. Environmental Protection Agency,
    Standards of Performance for  Lime
    Plants, CFR Part 60,  page 9472,
    March 7,  1978.
 3.  Hyer Industries, Inc. Thayer R.F. —A
    Belt  Scale of Proven Stability in
    Severe Environments, Bulletin 5D66
    Rev-1,  1977.
 4.  Ramsey Engineering Co., Ramsey
    Precision  Belt Scale System Model
    10-14, Bulletin TDS 10-14/40-17REV,
    1979.
 5. Kurylchek, A.L. "Belt  Conveyor
    Scales and Weigh Feeders," Process
    Instruments and Controls Handbook,
    Douglas M. Considine (Editor), McGraw
    Hill  Book  Company, Second Edition,
    pages 732-738,  1974
 6. National Bureau of Standards. Speci-
    fications, Tolerances, and Other
    Technical Requirements for Weighing
    and Measuring Devices, NBS Hand-
    book 44, September 1980.
 7. Pike,  C.E.  Requirements for the
    Approval  of Belt Conveyor  Scales,
    Southern Weighing and Inspection
    Bureau, Circular 9585-5, June 1971.
 8. Ted Houseconnect, Fuller Inc., per-
    sonal  communication  with  J.
    Richards, Engineering-Science,
    December 14, 1982.
 9. Karl Middour, Gifford-Hill, personal
    communication  with R. Segall, En-
    gineering-Science, December 6,
    1982.
10. Wallace & Tiernan Division, Pennwalt
    Corporation, Digital Weighbelt Feeder
    Series 31 -160, Catalog File 310.160,
    No Date.
11. Hyer  Industries, Inc.  Thayer  — A
    Weigh Feeder Designed for Comput-
    erized Plants, Bulletin 5D65-10/76-
    5M-SP, 1976.
12. Kay-Ray Inc., Digital  Weigh Scale
    Model 6000X, Bulletin 110-880, No
    Date.
13. Kay-Ray Inc., Weigh Scale Systems,
    Bulletin KR123-281, 1981.
14. Ohmart,  Weighart Series 4000,
    Bulletin SDBW-8177, No Date.
15. Kay-Ray Inc., On-Line Weigh Scale
    Model 6000, Bulletin  KR266-1081,
    No Date.
16. Ken Levin and Morris Yarrow, Ontario
    Cement, personal  communication
    with   J.   Richards,  Engineering-
    Science, December 13, 1982.
17. Charles, J., System Service Corpora-
    tion,  personal communication  to R.
    Segall, Engineering-Science, De-
    cember 8,  1982.
18. Milltronics Inc.,  Sankyo Flowmeter
    System Specification  Sheet  1051,
    No Date.
19. Yarway, Solids  Flow Transmitter,
    Bulletin 5M875C, No Date.
20. Wittmann,  J.P. Raw  Meal  Kiln
    Weigh Feeding  Systems, Polysius
    Corporation, October 1978.
21. Mueller, K., Polysius Corporation,
    personal communication with J.
    Richards,  Engineering-Science, De-
    cember 21, 1982.
22. Polysius Corporation, Dosier-System
    POLDOS, Bulletin 1240 DIE (6000
    BU), July 1979.
23. Polysius Corporation, Fordertechnik,
    Dosier-System  POLDOS,  Bulletin
    1247 <3,5679FM), No Date.
24. Levine,  S. High-Value End  Uses
    Underlie Plant Design, Pit & Quarry,
    pages 53-56 and 123, May 1980.
25. Trauffer,  Walter E. Recent  Plam
    Improvement Program Gives Austir
    White Lime Well  Balanced Operation

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    Pit & Quarry, pages 106-110, May
    1965.
26. Gori, T., and Schwarzkopf, F. Metal-
    lurgical and Chemical Lime Production
    via a Coal-Fired Preheater System,
    Pit & Quarry,  pages 100-104, June
    1979.
27. Sklavwer, M.M.,  and Yearham,  B.
    Preheater Cuts Heat Input Demand,
    Pit & Quarry, pages 52-55,  May
    1979.
28. No Author.  Parallel Flow Lime Kiln
    Lower As Heat Consumption, Pit &
    Quarry, pages 85-87, May 1981.
29. Trauffer, Walter E., Peerless'  New
    Detroit  Plant,  Pit & Quarry, Volume
    84, pages 84-93, July 1972.
30. Liptak, B. G. (Editor). Magnetic Flow-
    meters, Instrument Engineers' Hand-
    book, Volume  I — Process Measure-
    ment, pages 478-487, Chilton Book
    Company, 1969.
31. Webb,  A. S. Electromagnetic Flow-
    metering  ...  Basics, Products, and
    Applications; Instrumentation Tech-
    nology, Volume 21, Number 3, pages
    29-36,  March 1974.
32. Grzenda, J.H., Foxboro Corporation,
    personal  communication  with  R.
    Segall, Engineering-Science, De-
    cember 9, 1982.
33. Liptak, B.C. (Editor). Instrumentation
    in the Processing Industries, Chilton
    Book Company, 1973.
34. Harrison, R. Flow Measurement — A
    State of the Art Review, Chemical
    Engineering, Volume 87, Number 1,
    pages 97-104, January 14,  1980.
R.  R. Segall and J.  R. Richards are with Engineering-Science,  Durham, NC
  27701.
Thomas J. Logan is the EPA Project Officer (see below).
The complete report, entitled "Technical Assistance Document: Quality Assur-
  ance Guideline for Process Feed Rate Monitors in the Portland Cement and
  Lime Industries,"(Order No. PB84-101 468; Cost: $1O.OO, subject to change)
  will be available only from:
        National Technical Information Service
        5285 Port Royal Road
        Springfield.  VA 22161
        Telephone: 703-487-4650
The EPA Project Officer can be contacted at:
        Environmental Monitoring Systems Laboratory
        U.S. Environmental Protection Agency
        Research Triangle Park, NC 27711
                                                                          •&U. S. GOVERNMENT PRINTING OFFICE: 1983/759-102/0800

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United States
Environmental Protection
Agency
Center for Environmental Research
Information
Cincinnati OH 45268
Official Business
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