TD1064 United States Office of June 1989 /" „ ,
JJ33 Environmental Protection Solid Waste "•> ' |, ^ \
' Q Agency Washington, D C. 20460 '-~-EPA Background Document For
Second Third Wastes To
Support 40 CFR Part 268
Land Disposal Restrictions
Final Rule
Second Third Waste Volumes,
Characteristics, and Required and
Available Treatment Capacity
Volume 1 1
OOOR89104B
*>n v
WAST!F. :v1AN.\GLWEN7 DIVISION
OFFICE OF THE DIRECTOR
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"PL/ /it if'I
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BACKGROUND DOCUMENT
FOR
SECOND THIRD WASTES TO SUPPORT 40 CFR
PART 268 LAND DISPOSAL RESTRICTIONS
FINAL RULE
SECOND THIRD WASTE VOLUMES, CHARACTERISTICS,
AND REQUIRED AND AVAILABLE TREATMENT CAPACITY
Volume II
U.S. Environmental Protection Agency
Office of Solid Waste
401 M Street, S.W.
Washington, D.C. 20460
June 8, 1989
U S Environmental Protection Agency
Region 5, Library (PL-12J)
77 West Jackson Boulevard, IZtn HOOT
Chicago, It 60604-3590
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TABLE OF CONTENTS
Section Page No.
Volume I
EXECUTIVE SUMMARY E-l
1.0 INTRODUCTION 1-1
1.1 Legal Background 1-1
1.1.1 General Requirements Under HSWA 1-1
1.1.2 Schedule for Developing Restrictions 1-1
1.1.3 Variance from the Schedule 1-3
1.2 Summary of Previous Land Disposal Restrictions 1-4
1.2.1 Solvents and Dioxins 1-4
1.2.2 California List 1-6
1.2.3 First Third Wastes 1-8
1.2.4 Underground Injected Wastes 1-9
1.3 Introduction to the Second Thirds Final Rule 1-12
1.3.1 Summary of the Second Thirds Proposed Rule 1-12
1.3.2 Response to Major Capacity Related Comments
on the Second Thirds Proposed Rule 1-18
1.3.3 Major Revisions to the Second Thirds Final Rule . 1-20
2.0 CAPACITY ANALYSES RESULTS 2-1
2.1 General Methodology 2-1
2.1.1 Data Set Development 2-1
2.1.2 Capacity Analysis Methodology 2-10
2.2 Results 2-15
2.2.1 All RCRA Wastes 2-15
2.2.2 Solvents 2-18
2.2.3 NonSolvent RCRA Wastes Containing
Halogenated Organic Compounds (HOCs) 2-22
2.2.4 First Third Wastes 2-26
2.2.5 Underground Injected Sol vent Wastes 2-35
2.2.6 Underground Injected California List Wastes 2-38
2.2.7 Underground Injected First Third Wastes 2-41
2.2.8 Determination of Available Capacity for Second
Third Final Rule 2-46
2.2.9 Second Third Promulgated Wastes 2-50
2.2.10 Waste Code-Specific Capacity Analyses for
Second Third Promulgated Wastes (Nonsoils) 2-67
2.2.11 Contaminated Soils 2-133
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TABLE OF CONTENTS (continued)
3.0 CAPACITY ANALYSIS METHODOLOGY.
Page No.
3-1
3.1 Determination of Required Treatment Capacity 3-1
3.1.1 Waste Volumes Affected 3-1
3.1.2 Treatability Analysis 3-6
3.2 Determination of Available Treatment Capacity 3-13
3.2.1 Determination of Combustion Capacity 3-14
3.2.2 Determination of Other Treatment
System Capacities 3-19
3.2.3 Development of the Treatment Capacity
Data Set and Results 3-36
3.3 Capacity Analysis (Comparison of Required and
and Available Treatment Capacity) 3-42
4.0 BIBLIOGRAPHY
4-1
Volume II
APPENDICES
Appendix A - F006 Analysis in Support of the Second Third
Final Rule A-l
Appendix B - Reanalysis of Sludge Combustion Capacity
Requirements for Wastewater Treatment Sludges
at DuPont's Chambers Works Facility B-l
Appendix C - Raw Data Used for Capacity Analysis C-l
Appendix D - Capacity Analysis for Second Third Promulgated
Wastes D-l
Appendix E - Waste Volume and Characterization Data for
Underground Injected KQ09 and K010 Waste Used
to Support the Second Third Final Rule E-l
Appendix F - Capacity Analysis for Contaminated Soil Wastes F-l
Appendix G - Alternative Treatment/Recovery Technology Groups .... G-l
Appendix H - Alternative Treatment/Recovery Technologies H-l
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APPENDIX A
F006 Analysis in Support of
the Second Third Final Rule
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APPENDIX A
TABLE OF CONTENTS
INTRODUCTION ,
1 . 1 Background
DATA SOURCES
2 . 1 TSDR Survey ,
2 . 2 Generator Survey
2.3 Data from Public Comments ,
Page No.
A-l
A-l
A-2
A-2
A-3
A-4
3. RESULTS A-5
3.1 TSDR Survey A-5
3.2 Generator Survey A-5
3.3 Data from Pub! i c Comments A-10
4. CONCLUSIONS A-12
Attachment A-l
Attachment A-2
Attachment A-3
LIST OF TABLES
Table A-l Analysis of F006 Generation at RCRA-Permitted
and Interim Status Facilities A-6
Table A-2 Summary Information for Generator Facilities of F006
Exceeding the Revised Cyanide Standards With Only
Exempt Hazardous Waste Treatment Onsite A-9
Table A-3 Summary of Information for Those TSDR Facilities
Generating F006 Exceeding the Revised Cyanide
Standards A-ll
Table A-4 Summary of Cyanide Concentration Data Supporting
the F006 Analysis A-13
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1. INTRODUCTION
1.1 Background
For the Second Third proposed rule, EPA proposed treatment standards
for cyanides in F006 nonwastewaters. The treatment standards were based
on the performance of wet air oxidation or alkaline chlorination followed
by chemical precipitation, settling, and filtration. EPA received many
public comments indicating that the proposed cyanide treatment standards
for F006 nonwastewaters were not achievable. New performance data on the
pretreatment of cyanides by alkaline chlorination also became available
to EPA after the original proposal of the rule, and the Agency has
evaluated those data. Based on this evaluation, EPA has significantly
raised the F006 cyanide treatment standards for the Second Third final
rule (from 110 mg/kg total cyanides and 0.064 mg/kg amenable cyanides to
590 mg/kg total cyanides and 30 mg/kg amenable cyanides). The cyanide
treatment standards to be promulgated are based on the performance of
alkaline chlorination followed by chemical precipitation, settling, and
filtration.
Many commenters also disputed EPA's belief that F006 wastes did not
contain cyanide levels above the treatment standards because they were
being pretreated for cyanides and therefore would not require commercial
cyanide treatment capacity.
In response to comments on capacity requirements for cyanide
treatment, EPA performed an analysis to estimate the volume of generated
F006 wastes that may exceed the promulgated cyanide treatment standards
and therefore require treatment for cyanides. EPA relied on two major
A-l
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data sources for this analysis: (1) the National Survey of Hazardous
Waste Treatment, Storage, Disposal, and Recycling Facilities (the TSDR
Survey), upon which capacity and volume determinations for the land
disposal restrictions are now based, and (2) the National Survey of
Hazardous Waste Generators (the Generator Survey), a new and
comprehensive source of detailed waste characterization data that is now
available on a limited basis. EPA also evaluated data submitted by
several commenters on cyanide concentrations in F006 waste streams.
Section 2 of this Appendix presents a more detailed discussion of the
data sources used and the approach taken in evaluating the available data
in order to quantify the volumes of generated F006 that may exceed the
revised cyanide treatment standards. Section 3 presents discussions and
data tables on the results of the analysis. Section 4 presents the
conclusions.
2. DATA SOURCES
2.1 TSDR Survey
The TSDR Survey was designed as a census of RCRA-permitted and
interim status treatment, disposal, and recycling facilities, with no
weighting factors for statistical analyses to project national capacity
estimates. The survey also included a sample of storage-only
facilities. The responses to the survey have undergone extensive
technical review and QA/QC, thus providing a comprehensive source of data
on land disposed waste volumes and treatment, recovery, and disposal
capacity.
A-2
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EPA screened the TSDR Survey capacity data base to identify the
facilities that generated F006 and those that also had alkaline chlori-
nation or another cyanide treatment onsite. It was assumed that these
facilities were treating or were able to treat their cyanide wastes
onsite to meet the cyanide standards and would not need commercial
cyanide treatment capacity. The TSDR Surveys for the remaining TSDR
facilities identified as generating F006 were evaluated to determine
which ones generate noncyanide F006 wastes (e.g., facilities that perform
chrome electroplating and therefore do not use cyanide in their
process). The F006 waste streams from these facilities were assumed not
to require commercial cyanide treatment capacity.
As a worst-case scenario, EPA assumed that the remaining F006 waste
streams (cyanide-bearing F006 wastes generated at TSDR facilities that
did not have onsite cyanide treatment) have cyanide concentrations above
the revised treatment standards.
2.2 Generator Survey
EPA recently conducted the National Survey of Hazardous Waste
Generators (the Generator Survey). The Generator Survey was designed to
gather data on waste generators and exempt hazardous waste treatment
capacity, and it includes detailed waste characterization data. Although
the majority of these data are not yet available, EPA used a subset of
the data to evaluate the amount of treatment capacity required by
electroplating wastes, i.e., F006 waste streams.
Data available for the F006 analysis included about 550 Generator
Surveys from facilities not having a RCRA permit or interim status but
with exempt hazardous waste treatment capacity onsite (non-TSDRs). This
A-3
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limited subset of Generator Surveys was screened to identify facilities
that reported generating F006 waste streams. Data were then gathered on
the volumes and characteristics of each F006 waste stream, including the
reported cyanide concentrations. The reported cyanide concentrations
were assumed to be total cyanides.
The Agency also reviewed waste characterization data from the
Generator Survey for about 950 TSDR facilities with land disposal or
commercial treatment/recovery operations. The data were screened to
quantify the volumes and characteristics of each generated F006 waste
stream, including the reported cyanide concentrations. The reported
cyanide concentrations were assumed to be total cyanides.
2.3 Data from Public Comments
In the public comments for the Second Third proposed rule, the Agency
received data from two commenters on cyanide concentrations in F006 waste
streams. The data supplied by one commenter, the National Association of
Metal Finishers, included data from PDC Laboratories, Inc., on the total
cyanide concentrations in 88 F006 waste stream samples from a variety of
generators.
The other commenter, United Technologies (Pratt & Whitney), supplied
total and amenable cyanide concentration data on samples from F006 wastes
generated at two of its facilities.
A-4
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3. RESULTS
3.1 TSDR Survey
The analysis of TSDR Survey data showed that 104 million gallons of
F006 were generated in 1986 at 358 TSDR facilities. (This volume does
not include F006 wastes generated at facilities not having a RCRA permit
or interim status, i.e., non-TSDRs.) Of this 104 million gallons,
72 million gallons (69 percent) were generated at facilities that have
onsite cyanide treatment and therefore were assumed to be treating or
able to treat their wastes to meet the cyanide standards, and 28 million
gallons (27 percent) did not contain cyanides. Only 4 million gallons (4
percent) of F006 wastes were generated at these facilities that may, as a
worst-case scenario, contain cyanide concentrations above the revised
treatment standards. A summary of the F006 analysis conducted using the
TSDR Survey capacity data base is presented in Table A-l.
3.2 Generator Survey
Review of the subset of 550 Generator Surveys from non-TSDR facilities
resulted in the identification of 184 facilities generating F006 waste
streams. The total volume of F006 waste streams generated at these
facilities in 1986 was 14 million gallons. Of this 14 million gallons,
12.7 million gallons (91 percent) were reported as not containing
cyanides or as having cyanide concentrations below the revised total
cyanide treatment standard; 0.5 million gallons (less than 4 percent)
were reported as being of unknown cyanide content; 0.5 million gallons
(less than 4 percent) were reported to contain cyanides, but at unknown
A-5
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5758s
Table A-l Analysis of F006 Generation at RCRA-Permitted
and Interim Status Facilities
Category
Facilities with
onsite cyanide
treatment
Percent of Generated
Number of total no. of volume
facilities facilities (million gallons)
142 40 72
Percent
of total
generated
69
Facilities generating 114 32 28 27
noncyanide F006
Facilities generating 102 28 44
F006 with cyanide
concentrations that
may be above the
revised treatment
standards ___ ___
TOTAL 358 100 104 100
Source: TSDR Survey.
A-6
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concentrations; and 0.2 million gallons (1.4 percent) were reported to
have cyanide concentrations above the revised total cyanide treatment
standard.
The generators of the four waste streams included in the 0.2 million
gallons of F006 reported to have cyanide concentrations above the revised
total cyanide treatment standard were contacted for information on their
F006 waste streams. One facility had ceased all cyanide plating
operations (and F006 generation) in January 1989 because of the
requirements of the First Third final rule. The other three facilities
specifically mentioned the presence of ferrocyanide complexes in their
F006 waste streams as the reason for the high cyanide concentrations.
Based on information in the Generator Survey for non-TSDR facilities,
it is estimated that only 0.8 million gallons (6 percent) of the F006
waste generated at these facilities may have cyanide concentrations above
the revised treatment standards. This percentage is taken from the
volume of F006 waste streams reported to contain cyanides, but at an
unknown concentration, and from the F006 waste streams reported to have
cyanide concentrations above the revised treatment standards. The
percentage of F006 wastes for which it was reported that the cyanide
content was unknown was assumed not to have cyanide concentrations above
the revised treatment standards. It is believed that if these waste
streams had cyanide concentrations above the standard, the generators
would at least know that cyanides were present. Summary information for
those non-TSDR generator facilities with F006 wastes exceeding the
A-7
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revised cyanide standards is presented in Table A-2. Additional data for
all non-TSDR facilities evaluated as part of this analysis are contained
in Attachment A-l.
From the Generator Survey data for the subset of TSDR facilities, 138
facilities generating F006 waste streams were identified. The volume of
F006 waste streams generated at these facilities in 1986 was
approximately 82 million gallons. Of the 82 million gallons generated in
1986, 76 million gallons (93 percent) were reported as not containing
cyanides or as having cyanide concentrations below the revised total
cyanide treatment standard; 6 million gallons (7 percent) were reported
as being of unknown cyanide content; less than 0.6 million gallons (less
than 1 percent) were reported to contain cyanides, but at an unknown
concentration; and 0.1 million gallons (less than 1 percent) were
reported to have cyanide concentrations above the revised total cyanide
treatment standard.
Based on these data, it is estimated that less than 0.7 million
gallons (less than 1 percent) of the F006 waste generated at these
facilities may contain cyanide concentrations above the revised treatment
standards. This percentage is taken from the volume of F006 waste
streams reported to contain cyanides, but at unknown concentrations, and
from the F006 waste streams reported to have cyanide concentrations above
the revised treatment standards. The percentage of F006 wastes for which
it was reported that the cyanide content was unknown was assumed not to
have cyanide concentrations above the revised treatment standards. It is
believed that if these waste streams had cyanide concentrations above the
A-8
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5758s
Table A-2 Summary Information for Generators of F006 Exceeding
the Revised Cyanide Standards with Only
Exempt Hazardous Waste Treatment Onsite
Facility name
volume
EPA ID number generated
Reported
cyanide
concentration
(ppm)
Comment
Amercord
GAD008966400 782 T
(187.680 g)
10,000 Waste reported to contain
ferrocyanide complexes;
facility has alkaline
chlorination onsite
American Plating
PAD990752099
182 T
(43,680 g)
<1,000 Waste reported to contain
ferrocyanide complexes;
facility has alkaline
chlorination onsite
LRC Electronics
NYD002204543
32 T
(7,680 g)
<1,000 Waste reported to contain
ferrocyanide complexes,
facility has alkaline
chlorination onsite
Shakerproof Div. ICYD990876252 41 T
of Illinois Tool (9,840 g)
1,000-5,000 Facility stopped generating
F006 in January 1989
Ajax Stamping & Mfg. PA0002346088 550 T
(132,000 g)
Unknown* Waste reported to be shipped
offsite; facility has
alkaline chlorination onsite
Perko Inc
FLD004117077 300 T
(72,000 g)
Unknown* Waste reported to be shipped
offsite; facility has
alkaline chlorination onsite
6E, Somersworth
NHD001091073 158 T
(37,920 g)
Unknown* Waste reported to be shipped
offsite; facility has
alkaline chlorination onsite
Waterbury
Companies, Inc.
CTD001165695
131 T
(31,400 g)
Unknown* Waste reported to be shipped
offsite; facility has cyanide
oxidation onsite
Sheller-Globe Corp. IND006066377
1.064 T
(255,360 g)
Unknown* Waste reported to be shipped
offsite; facility has
electrochemical cyanide
oxidation onsite
TOTAL
3.240 T
(0.8 Mgal)
Source: Generator Survey - sample of approximately 550 surveys from generator facilities with only exempt
capacity onsite, i.e., non-TSDRs.
* Facilities reported that these waste streams contain cyanides, but at an unknown concentration.
T = tons g = gallons Mgal = million gallons
A-9
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standard, the generators would at least know that cyanides were present.
Summary information for those TSDR facilities generating F006 wastes
exceeding the revised cyanide standards is presented in Table A-3.
Additional data for all the TSDR facilities generating F006 wastes that
were evaluated as part of this analysis are contained in Attachment A-2.
The combined results of the two Generator Survey analyses identified
322 facilities generating F006. The total volume of F006 waste streams
generated at the facilities in 1986 was 96 million gallons. Of this
96 million gallons, 89 million gallons (93 percent) were reported as not
containing cyanides or as having cyanide concentrations below the revised
total cyanide treatment standard; 7 million gallons (7 percent) were
reported either as being of unknown cyanide content, to contain cyanides
at unknown concentrations, or to have cyanide concentrations above the
revised total treatment standard. However, generators reported that less
than 1.6 percent of the volume of F006 wastes at these facilities have a
cyanide concentration above the treatment standard or had cyanides with
unknown concentration levels. In addition, several of the facilities
with unknown cyanide concentrations have onsite cyanide treatment. If it
is assumed that these waste streams would meet the BOAT standard, then
less than 0.7 percent of the F006 wastes from Generator Survey facilities
would require cyanide treatment capacity.
3.3 Data from Public Comments
Evaluation of the commenter-supplied data shows that, of the 88 waste
streams reported by the National Association of Metal Finishers (data
from PDC Laboratories, Inc.), only 8 waste streams (9 percent) had total
A-10
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5758s
Table A-3 Sunmary of Information for Those TSOR Facilities
Generating F006 Exceeding the Revised Cyanide Standards
Facility EPA
ID number
CTD001168137
GAD075920801
KYD044914356
PAD002344315
TND069080513
WID980704209
CTD0058865072
NYD001325661
PA0002344315
TXD030171979
PAD002346088
Waste
description
"Dry" metal hydroxide
solids not "fixed"
Waste exactly as
described
Waste exactly as
described
Other wastewater
treatment sludge
Waste exactly as
described
Solidified treatment
residue
Waste exactly as
described
Lime sludge with metals/
metal hydroxide sludge
Inorganic solid
Waste exactly as
described
Lime sludge with
metals/metal hydroxide
sludge
TOTAL
Volume Reported cyanide
generated concentration (ppm)
66 T 625
(15.940 g)
94 T 640
(22,560 g)
100 T 5,000
(24.000 g)
15.6 T 698
(3.744 g)
169 T 5,000
(40,560 g)
45 T 630
(10.800 g)
200 T Unknown*
(48,000 g)
110 T Unknown*
(26.400 g)
1,556 T Unknown*
(373,440 g)
2 T Unknown*
(480 g)
550 T Unknown*
(132.000 g)
2,908 T
(0.7 Mgal)
Comment
Waste sent off site for
stabilization and landfill
Waste underwent onsite alkaline
chlonnation
Waste underwent onsite alkaline
chlorination
Waste sent off site for landfill
Waste underwent onsite alkaline
chlorination
Waste sent off site for landfill
Waste sent offsite for landfill
Waste sent offsite for landfill
Waste sent offsite for landfill;
facility has alkaline
chlonnation onsite
Waste sent offsite for landfill
Waste sent offsite for landfill
Source: Generator Survey - for data for approximately 950 permitted TSOR facilities.
* These facilities reported that these waste streams contain cyanides, but at an unknown concentration.
T = tons
g = gallons
Mgal = million gallons
A-ll
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cyanide concentrations above the revised treatment standard. Waste
stream volume information was not supplied by the commenter. Upon review
of the data supplied by United Technologies (Pratt & Whitney), the Agency
found that none of the 47 samples for which data were supplied had total
cyanide concentrations above the revised treatment standard, and only 2
out of the 47 samples (4 percent) had amenable cyanide concentrations
above the revised treatment standard. One sample reported by the
commenter was not considered by the Agency. This sample was assumed to
be erroneously reported because the amenable cyanide concentration was
greater than the total cyanide concentration. Waste stream volume
information was not supplied by this commenter.
4. CONCLUSIONS
A summary of the cyanide concentration data from the Generator Survey
and commenter information used to support the F006 analysis is presented
in Table A-4. Although only data from a subset of F006 generators have
been evaluated, it is believed that these data establish that only a
small percentage of all F006 wastes will have cyanide concentrations
above the revised treatment standards (i.e., only a small percentage of a
volume of F006 wastes with cyanides and without cyanides). If EPA
considered only the volumes of F006 wastes that had cyanides, the percent
of wastes that would exceed the standard would obviously increase.
However, the volume of the land disposed waste includes all F006 wastes
land disposed (i.e., volumes with and without cyanides). Thus, the
A-12
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appropriate percentage for determination of the volume of land disposed
waste that would exceed the standard is the percentage of all F006 wastes
that exceed the standards. The data from the TSDR Survey, Generator
Survey, and commenters consistently indicate that the percentage of all
F006 wastes that may exceed the standard is small, ranging from a low of
about 1 percent to a high of about 10 percent. As a worst-case scenario,
it is estimated that 10 percent of F006 wastes generated may have cyanide
concentrations above the revised treatment standards.
For the First Third final rule, EPA estimated that 129 million
gallons per year of land disposed F006 wastes require alternative
treatment. Using the assumption that the percentage of generated F006
waste that contains cyanide concentrations above the treatment standards
is representative of the percentage of land disposed F006 waste that
contains cyanide concentrations above these standards, the Agency
estimates, as a worst-case scenario, that 10 percent of the 129 million
gallons of F006 waste land disposed, or about 13 million gallons per
year, will require alternative commercial treatment capacity for
cyanides. Sufficient alkaline chlorination capacity (46 million gallons
per year) exists to treat this volume of waste.
A-14
-------
ATTACHMENT A-l
Analysis of TSDR Survey Data of F006 Generation
A-15
-------
Attachment A-la
This attachment contains a computer printout showing the facilities
that were identified by the TSDR Survey as generating F006. The printout
presents facility name, facility ID number, and all waste codes contained
in the waste stream. The printout also presents the volume generated and
the type of cyanide waste stream as determined by analysis of the TSDR
Survey data.
Key:
Type of cyanide waste stream
A - Facility has onsite cyanide treatment
B - Waste assumed to require offsite treatment for cyanides
C - Waste assumed not to contain cyanide
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Attachment A-lb
This attachment contains a table showing the results of an analysis
to confirm and update the reported F006 generation volumes. The table
presents the facility name and EPA ID number, the original volume
reported in the TSDR (gallons), and the corrected volume following the
analysis. Finally, for each waste stream that was revised, the table
gives a reason for the revision.
A-45
-------
Attachment A-lb Results of Evaluation of Reported
Generation Volumes for F006 Wastes
Facil ity name/
EPA ID number
Reported
volume
(gallons)
Corrected
volume
(gallons)
Reason
Motorola Inc. 20,666,135
Government Ele.
AZD008399636
Hughes Aircraft Co. 14,743,000
CAD041666819
Westinghouse Electric 17,400,000
Corp. Bryant Div.
CTD001183078
WHYCO Chromium Co. Inc. 17,280,000
CTD001450154
Bussman Cooper Industries 2,295,000
CTD042308270
Susan Bates Inc. 2,400,000
CTD080848666
GMC CPC Group 142,444,609
Lakewood Plant
GAD059522870
Shaefer Eaton Plant #1 7,500,000
IAD005267745
GE Switchgear Operations 7,983,838
IAD005272703
Sloan Valve 9,736,590
ILD005121033
0 Volume reported was
influent to waste-
water treatment
720 Volume reported was
influent to waste-
water treatment
70,320 Volume reported was
influent to waste-
water treatment
0 Volume reported was
prior to sludge
dewatering
0 Volume reported was
influent to waste-
water treatment
0 Volume reported was
influent to waste-
water treatment
0 Volume reported was
influent to waste-
water treatment
0 Volume reported was
influent to waste-
water treatment
0 Volume reported was
influent to waste-
water treatment
0 Volume reported was
influent to waste-
water treatment
A-46
-------
Attachment A-lb (continued)
Facility name/
EPA ID number
Reported
volume
(gallons)
Corrected
volume
(gallons)
Reason
Amerock Corp.
ILD005163332
GE Morrison
ILD005272992
Roll Coater Inc.
IND006420087
Midwest Steel Co.
IND016584641
CMC Fisher Guide Div.
IND980700801
Balfour L.G. Foundation
MAD001199256
Westford Anodizing Corp.
MAD062173497
Rosemar Silver Co.
MAD080812431
Michigan Disposal
MID000724831
GMC Detroit Diesel
MID005356803
Chem-Met Services Inc.
MID096963194
65,000,000
27,406,000
45,360,000
72,450,300 2,640,000
140,837,040
7,170,815
6,375,000
2,500,000
24,420,240
51,100,000
18,520,000
9,840
0
0
Volume reported was
influent to waste-
water treatment
Volume reported was
influent to waste-
water treatment
Volume reported was
influent to waste-
water treatment
Volume prior to
dewatering
Volume reported was
influent to waste-
water treatment
Volume reported was
influent to waste-
water treatment
Volume reported was
influent to waste-
water treatment
Volume reported was
influent to waste-
water treatment
Waste received from
offsite
Volume reported was
influent to waste-
water treatment
Waste received from
offsite
A-47
-------
Attachment A-lb (continued)
Facility name/
EPA ID number
Reported
volume
(gallons)
Corrected
volume
(gallons)
Reason
True Temper Sports Div. 50,000,000
MSD054531215
Stewart-Warner Corp. 12,349,000
NCD024895864
Data General Corp. 5,200,000
NCD086330412
DuPont E.I. De Nemours 16,266,000
Chambers Works
NJD002385730
CMC Delco Products Div. 2,240,640
OHD004255410
GMC Delco Moraine Div.
OHD045557766
Erieway Pollution Control
OHD055522429
U.S. Army Tobyhanna Depot
PA5213820892
Mill Service Inc. 42,000,000
PAD059087072
Waste Conversion 9,739,920
PAD085690592
Lockheed Georgia Co. 7,255,000
Charleston Plant
SCD048372023
1,987,200
1,702,320
3,544,800
4,328,264
0
0
0
0
Volume reported was
influent to waste-
water treatment
Volume reported was
influent to waste-
water treatment
Volume reported was
influent to waste-
water treatment
Waste received from
offsite
123,120 Volume reported was
volume after mixing
with nonhazardous
waste
Volumes reported
mid-treatment
Volume received from
offsite
Volume reported was
influent to waste-
water treatment
0 Wastes received from
offsite
0 Wastes received from
offsite
0 Volume prior to
dewatering
A-48
-------
ATTACHMENT A-2
Analysis of Generator Survey Data
from Non-TSDR Facilities
A-49
-------
Attachment A-2a
The attached table presents the data extracted from Generator Surveys
of facilities with only exempt treatment or recovery processes onsite,
i.e., non-TSDRs. For each waste stream, the table presents: the
facility name and EPA ID number; the waste code(s); the waste description
code(s) (see Attachment C-2 to Appendix C); the quantity generated (T =
tons, G = gallons); the onsite process codes through which the waste
went; whether or not the waste was shipped offsite; the reported cyanide
concentration (DK = does not know if cyanides are present; ? = cyanides
are present but at unknown concentration; NP = cyanide is not present in
the waste; NA = the constituent is not applicable to the waste stream);
the basis for the data (1 = based on testing and 2 = an estimate); and
information on whether the facility is discharging to a POTW or NPDES.
A-50
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Attachment A-2b
This attachment contains a table showing the results of an analysis
to confirm and update the reported generation volumes. The table
presents the facility name and EPA ID number, the original volume
reported in the Generator Survey (in gallons), and the corrected volume.
Finally, for each waste stream that was revised, the table gives a reason
for the revision.
A-90
-------
Attachment A-2b Results of Evaluation of Reported
Generation Volumes for Non-TSDR Facilities
Facility name/
EPA ID number
Reported
volume
(gallons)
Corrected
volume
(gallons)
Reason
Milwaukee Plating
WID006090187
GTE Products
PAD003050846
Maxwell Communication
TND980559702
Ford Motor Co. Saline PH.
MID009305655
Quality Electroplating Corp.
PRD090592544
Ajax Stamping and Mfg.
PAD002346088
Summit Finishing
IND067879106
Thomson Consumer Electronics
IND006932305
Fairchild Weston Systems
FLD083200998
BOC Group Leeds Plant
MOD000822668
Scovill Inc.
GAD003480530
11,792,000
37,964,160
13,560
1,084,800
11,
700,
39,
1,531,
1,430,
992,
878,
319,
12,483,
760
000
120
200
000
160
214
241
545
0
0
0
90,000
26,400
0
166,500
Volume reported was
influent to waste-
water treatment
Volume reported was
influent to waste-
water treatment
Volume reported was
influent to waste-
water treatment
Volume reported was
influent to waste-
water treatment
Volume reported
prior to dewatering
Volume reported
prior to dewatering
Volume reported
prior to dewatering
Volume reported
prior to dewatering
Volume reported
prior to dewatering
Volume reported
prior to dewatering
Volumes reported
mid-treatment
A-91
-------
ATTACHMENT A-3
Analysis of Generator Survey Data from TSDR Facilities
A-92
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Attachment A-3a
This attachment contains a computer printout showing Generator Survey
data on TSDR facilities with RCRA-permitted or interim status treatment,
storage, disposal, or recovery operations onsite. The printout presents
the facility ID number, the waste stream number, the cyanide waste codes
in the group, and the 1988 volumes generated. The table also presents
the 1986 quantity generated and the unit of measure (T = tons, G =
gallons). Finally, the table presents cyanide concentration data (-1 =
bad data; -3 = not applicable; -4 = don't know concentration; -8 =
present, but concentration unknown; and -9 = constituent not present)
and the basis for the data (1 = based on testing and 2 = estimate). The
printout also shows concentration data for other constituents; however,
these data were not used in this analysis.
A-93
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Attachment A-3b
This attachment contains a table showing the results of an analysis
to confirm and update the reported generation volumes. The table
presents the facility EPA ID number, the original volume reported in the
Generator Survey (in gallons), and the corrected volumes. Finally, for
each waste stream that was revised, the table gives a reason for the
revision.
A-109
-------
Attachment A-3b Results of Evaluation of Reported
Generation Volumes at TSDR Facilities (Generator Survey)
EPA ID number
CTD001183078
ILD006271696
IND016584641
IND980700801
MID005327580
MID005356860
OHD055522429
ORD089452353
PAD085690592
Reported
volume
(gallons)
68,500
10,255,200
72,451,440
1,373,520
10,368,000
136,880,000
3,544,800
3,955,440
3,105,120
636,000
4,320
10,928,400
Corrected
volume
(gallons)
70,320
0
2,640,000
0
0
0
0
0
0
0
0
0
Reason
Adjusted to match TSDR volume
Volume reported was influent
to wastewater treatment
Volume prior to dewatering
Volume reported was influent
to wastewater treatment
Volume reported was influent
to wastewater treatment
Volume reported was influent
to wastewater treatment
Waste received from offsite
Waste received from offsite
Waste received from offsite
Waste received from offsite
Waste received from offsite
Waste received from offsite
A-110
-------
APPENDIX B
Reanalysis of Sludge Combustion Capacity
Requirements for Wastewater Treatment
Sludges at DuPont's Chambers Works Facility
-------
Recent actions taken by EPA and by DuPont at its Chambers Works
facility in Deepwater, New Jersey, result in a significant change in
available capacity for sludge/solid incineration. A summary of the
current and proposed hazardous waste management operations relative
to this issue is presented below.
The landfill at the DuPont Chambers Works facility receives all
wastewater treatment sludges generated at that facility. These sludges,
as shown in Figure 1, include both the primary and secondary treatment
sludges generated by the wastewater treatment system. Prior to promulga-
tion of the Solvent and First Third LDRs, these wastewater (biological)
treatment sludges were considered to be mixed RCRA waste streams that con-
tained solvents (F001-F005) among their constituents. The sludges were
generated from the treatment of all hazardous wastewaters at this facili-
ty, including those wastewaters received from offsite and those generated
onsite. Leachate from the landfill was also treated in the wastewater
treatment system and, therefore, also resulted in the generation of
residual sludges.
At the time of promulgation for the Solvent and First Third final
rules, these wastewater treatment sludges (16 million gallons generated
per year) were determined to require alternative treatment as solvent
wastes because they were derived from solvent wastewaters (both the
wastewaters received from offsite and those generated onsite contained
solvents) and from landfill leachate (the leachate was from a landfill in
which solvent wastes had been disposed of; therefore, this leachate was
considered solvent waste in accordance with the "derived from" rule).
B-l
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These sludges were determined to require 16 million gallons of commercial
sludge combustion capacity during the capacity analysis for the Solvents
rule.
Since the Solvent and First Third rules were promulgated, DuPont has
taken steps intended to exempt its wastewater treatment sludges from regu-
lation under the Solvents portion of the LDRs. First, DuPont petitioned
for (and was granted) a de minimis exemption from EPA for the solvent
wastes it generated onsite at its Chambers Works facility. (See the
notice of petition, 54 FR 3132, for more information about DuPont's de
minimi's exemption petition for solvents generated onsite.) Second, the
facility has also stopped accepting solvent wastewaters from offsite for
treatment. These steps have essentially removed all solvents from the
primary wastewater treatment sludges except for those derived from the
treatment of landfill leachate.
Also, EPA has recently amended the schedule under the LDRs, assigning
multisource leachate wastes to the Third Third portion. Because of this
amendment, multisource leachate waste (and sludges derived from treatment
of such leachates) will not be subject to regulation under the LDRs until
May 1990. (See the final rule, 54 FR 8264, for more information about the
leachate amendment.) Therefore, the primary wastewater treatment sludges
at DuPont's Chambers Works facility are exempt from the LDRs until May
1990.
DuPont plans to continue to generate secondary wastewater treatment
sludges at its Chambers Works facility that contain solvents and require
incineration. These sludges will be sent offsite for incineration until
B-3
-------
an onsite carbon regeneration furnace (currently being modified to burn
these sludges) is operational. After they have been treated in the carbon
regeneration furnace, the residuals from treatment of this sludge (primar-
ily incinerator ash) are expected to meet BOAT standards for solvents
under the LDRs and can be disposed of in the onsite landfill. (Figure 2
presents the proposed wastewater treatment system and the proposed combus-
tion unit for the secondary treatment sludge at DuPont Chambers Works.)
Currently, according to data supplied by DuPont in its case-by-case
extension application, the quantity of secondary sludge routinely gener-
ated is much less than the quantity of primary sludge generated. (See
the attached Figure 3 and Table 1 from the "Chambers Works Case by Case
Extension Application, Hazardous Waste Land Disposal Restrictions of
November 8, 1988," dated June 1988.) Since a large majority (over 99 per-
cent) of the wastewater treatment sludges generated in 1986 (and assigned
to commercial sludge combustion capacity) were primary sludges, the sludge
combustion capacity currently required as alternative treatment by the
Chambers Works facility for secondary sludges (less than 1 million gallons
per year) can be considered insignificant for national capacity determina-
tions.
The primary wastewater treatment sludges generated by the DuPont
Chambers Works facility are still being sent to its onsite landfill for
disposal. The secondary treatment sludges will continue to be sent off-
site for incineration until the modified onsite carbon regeneration unit
is operational, at which time these sludges will be treated onsite.
Because the primary sludges meet the treatment standards for the First
B-4
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Figure 3
TOTAL VOLUME OF PRIMARY SLUDGE GENERATED
SLUDGE FIL
£)' MONTH
maximum filter capacity (vet basis)
•0 r -*
-*"•
\ ,' > ,-•' \..-*\ ,'
0 2 4 « 8 10 12 14 15 IB 20 22 24 « 23 30 32 34 35 33
SINCE JAN-U85
SLUDGE ('LESS SECONDS fir) EY MONTH
300-.
T
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HOMTHS SINCE J*N-158« -
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N
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B-b
-------
f
r
TABLE 1
PRIMARY SLUDGE GENERATED SINCE 1985
SLUDGE VOLUMES IN TONS/DAY
MONTH
JAN 1985
FEB 1985
MAR 1985
APR 1985
MAY 1985
JUN 1985
JUL 1985
AUG 1985
SEP 1985
OCT 1985
NOV 1985
DEC 1985
JAN 1986
FEB 1986
MAR 1986
APR 1986
MAY 1986
JUN 1986
JUL 1986
AUG 1986
SEP 1986
OCT 1986
NOV 1986
DEC 1986
JAN 1987
FEB 1987
.MAR 1987
APR 1987
MAY 1987
JUN 1987
JUL 1987
AUG 1987
SEP 1987 "
OCT 1987
NOV 1987
DEC 1987
JAN 1988
FEB 1988
MAR 1988
TOTAL
SLUDGE
211.96
233.54
176.63
223.94
207.88
257.63
214.00
250.68
227.10
169.50
198.67
212.64
195.99
166.98
180.03
202.53. -
219.77
186.38
187.50
191.24
202.18
172.22
199.37
243.21
196.67
227.90
199.73
214.81
225.21
224.99
272.08
260.87
274.13
330.17
325.38
264.61
320.66
328.31
266.99
PRIMARY
SLUDGE
211.96
233.47
175.61
223.90
207.88
257.07
213.25
249.87
226.29
168.72
198.53
212.20
195.25
166.60
180.03
202.32
219.77
186.24
186.96
191.03
202.00
172.15
199.16
243.07
196.50
227.90
199.73
214.81
225.21
223.80
271.23
259.28
272.48
328.94
324.53
263.01
319.64
326.09
265.02
SECONDARY
SLUDGE
0.00
0.08
1.02
0.04
0.00
0.56
0.75
0.82
0.81
0.78
0.14
0.44
0.75
0.38
0.00
0.21
0.00
0.14
0.54
0.20
0.18
0.07
0.21
0.14
0.17
0.00
0.00
0.00
0.00
1.19
0.85
1.60
1.65
1.22
0.84
1.60
1.02
2.22
1.97
b-7
-------
Third final rule and are no longer subject to the restrictions of the
Solvents final rule, the 16 million gallons of sludge combustion capacity
that was assigned to these sludges (because they were considered to
contain solvents) is now available for use as alternative treatment
capacity for wastes scheduled for restriction under the Second Third
final rule. However, the primary treatment sludges will be subject to
any restrictions placed on multisource leachate wastes by the Third Third
final rule in May 1990 and may require alternative treatment or recovery
capacity at that time.
B-8
-------
APPENDIX C
Raw Data Used for Capacity Analysis
-------
APPENDIX C
This appendix presents the TSDR Survey data used for the capacity
analysis for the Second Third promulgated wastes. The tables present the
following data fields on a waste stream-specific basis:
• EPA waste code
• WDESC = waste description code (a definition of each code has
been included as Attachment 2 to this appendix)
• FCID = facility EPA ID number
• Facility name
• BOOK = TSDR booklet (J = waste piles, K = surface impoundments,
L = landfills, M = land treatment, N = underground injection)
• RECTYPE and KEYLTR identify TSDR Survey question number for the
waste stream
• QTY8 = the quantity requiring alternative treatment (this
quantity is adjusted for the closure, replacement, or retrofitting
of surface impoundments)
• UOM = unit of measure (G = gallons, T = tons, M = million
gallons)
• TRD = treatability group (the alternative technologies
associated with each treatability group are contained in
Appendix G)
• ATR = alternative treatment/recovery technology code (the
technologies associated with each code are contained in Appendix H)
• AVAIL = identifies if the ATR is available onsite
C-l
-------
ATTACHMENT C-l
Waste Stream-Specific Data
C-2
-------
SURVEY !
0 "ROMULCA1 LU WASTLS
^ ONLY
Q M --
Sg::
K SOURCE
TH SECOr.
'J-CBI f'AC
DAT
hASTt STRtAMS W
NO
Volume Unit
MU ATRl ATM 2 ATR3 ATR4 ATRS assigned of
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0
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5710S/17
Aggregate CBI Data
Volume requiring alternative
treatment capacity
Waste code (gal)
F007 529,200
F008 559,200
F009 6,720
IC027 2,981,520
K115 79,680
P030 8,640
P094 240
U190 43.440
U223 58.800
r_ -
-------
ATTACHMENT C-2
Waste Description Codes
-------
WASTE DESCRIPTION CODES
These waste description codes were developed specifically for this survey to supplement the descriptions listec
with the RCRA and other waste codes. (These waste description codes are not regulatory definitions.)
WASTE DESCRIPTION CODES FOR HAZARDOUS WASTE DESCRIBED BY A SINGLE RCRA F, K. P, OR U WASTE CCC:
A01 Spent solvent (F001-FOOS. K086)
A02 Other organic liquid (FG01-F005. K096)
A03 Slill bottom (F001-F005. K086)
A04 Other organic sludge (F001-F005. K086)
AOS Wastewater or aqueous mixture
A06 Contaminated soil or cleanup residue
A07 Other F or K waste, exactly as described"
A08 Concentrated off-spec or discarded
product
AOS Empty containers
A10 Incinerator asn
A11 Solidified treatment residue
A12 Other treatment residue (specify in
"Facility Notes")
A13 Other untreated waste (specify in "Fat Jit1
Notes")
•"Exactly as described" means that the waste matches the description of the HCRA waste code.
WASTE DESCRIPTION CODES FOR HAZARDOUS WASTE DESCRIBED BY A SINGLE RCRA 0 OR X WASTE CODE OR
THAT DESCRIBED BY MORE THAN ONE RCRA OR X WASTE CODE
INORGANIC LIQUIDS—Waste that is primarily
inorganic ana ntghly fluid (e.g . aqueous), with
low suspended inorganic solids and low organic
content.
B01 Aqueous waste with low solvents
602 Aqueous waste with low other toxic
organics
B03 Spent acid with metals
804 Spent acid without metals
805 Acidic aqueous waste
806 Caustic solution with metals Out no
cyanides
BO? Caustic solution with metals and cyanides
808 Caustic solution with cyanides out no
metals
809 Spent caustic
810 Caustic aqueous waste
811 Aqueous waste with reactive sulfides
812 Aqueous waste with other reactives tag.,
explosives)
813 Other aqueous waste with high dissolved
sotids
814 Other aqueous waste with low dissolved
sends
815 ScruDDer water
816 Leacnate
817 Waste liquid mercury
813 Other inorganic liquid (sceciry in "Facility
Notes")
INORGANIC SLUDGES—Waste that is pnmar-
ily inorganic, with moderate-to-nigh water
content and low organic content; pumpaoie.
819 Ume sludge without metals
820 Ume sludge with metals/metal hydroxide
sludge
821 Wastewater treatment sluage with toxic
organics
822 Other wastewater treatment sludge
823 Untreated plating sludge Without cyanides
824 Untreated plating sludge with cyanides
825 Other sludge with cyanides
826 Sludge with reactive sulfides
827 Sludge with other reactivas
B28 Qeqraasing sludge with metal scale or
filings
820 Air pollution control device sludge (eg .
lly asn. wet scruPOer stuoge)
820 Sediment or lagoon dragoul contaminated
with orrjanics
831 Sediment or lagoon dragout contaminated
with inorganics only
832 Drilling mud
833 Asbestos slurry or sludge
834 Chloride or other brine sludge
B35 Other inorganic sludge (specify m
"Facility Notes")
INORGANIC SOLIDS—Waste that is primarily
inorganic and solid, with low organic content
and low-to-moaerate water content; not
pumpaoie.
836 Soil contaminated with organics
837 Soil contaminated with inorganics only
838 Ash. slag, or other residue from inciner-
ation of wastes
839 Olher "dry" ash. slag, or thermal
residue
840 "Dry" lime or metal hydroxide solids
chemically "fixed"
841 "Dry" lime or metal hydroxide solids not
"fixed"
B42 Metal scale, filings, or scrap
843 Empty or crushed metal drums or con-
tainers
844 Batteries or cattery pans, casings, cores
845 Spent solid filters or adsoroents
846 Asoestos sonds and deons
847 Metal-cyanide salts/chemicals
848 Reactive cyanide sails/chemicals
849 Reactive sulfide salts/chemicals
B50 Other reactive salts/chemicals
851 Olher metal salts/chemicals
852 Olher waste inorganic chemicals
853 Lab packs of old chemicals only
854 Lab packs of debns only
855 Mixed lab packs
856 Other inorganic solids (specify in
"Facility Notes")
INORGANIC GASES—Waste that is primarily
inorganic with a low organic content and is a
gas at atmospfienc pressure.
857 Inorganic gases
ORGANIC LIQUIDS—Waste that is primarily
organic and is highly fluid, with low inorganic
solids content and fow-io-moderate water
content
858 Concentrated solvent-water solution
859 Halogenated lag , chlorinated) solvent
B60 Nonhalogenated solvent
861 Haiogenated/nonhaiogenated soivnt
mixture
862 Oil-water emulsion or mixture
B63 Waste oil
864 Concentrated aqueous solution of otne;
organics
865 Concentrated phenolics
866 Organic paint, ink, lacquer, or varnsn
867 Adhesives or expoxies
B6S Paint thinner or petroleum distillares
869 Reactive or polymertzaoie organic iiquu
870 Other organic liquid (scscify m Fac;::tv
Notes')
ORGANIC SLUDGES—Waste (hat is pnrrarny
organic, with low-to-moaerate inorganic soiics
content anq water content; pumpaoie.
871 Still bottoms of naiogenateq (e c . crier
nated) solvents or other organic ' cuids
872 Still bottoms of nonhaiogenated
solvents or other organic 'iquias
873 Oilv sludge
874 Organic caint or nx siuccs
875 Heac.'.'ve or coivnen;2s:e crcar c:
876 flesins. tars or tarn/ s;udce
877 Biological treatment siuccs
878 Sewage or other untreated EICIOC cai
sluage
879 Other organic sludge (specify m
"Facility Notes')
ORGANIC SOLIDS—Waste that is primarily
organic ana solid, with low-to-moaerate
inorganic content and water content: net
pumpaoie.
880 Haloqenated pesticide solid
881 Nonhalogenated pesticide solid
882 Solid resins or potymenzeo organics
883 Spent carbon
884 Reactive organic solid
885 Empry liber or plastic containers
886 Lab packs of old chemicals only
887 Lab packs of debris only
888 Mixed lab pacxs
889 Other halogenated organic solid
890 Other nonhaiogenaieo organic ac:;d
ORGANIC GASES—Waste that is pnmar iy
organic with low-io-moderate inorganic -onier
and is a gas at atmospheric pressure
891 Organic gases
NOTE. A list of X waste codes was developed specifically for this survey These X codes are not official RCRA waste codes and should be used
ONLY for this survey.
C-4U
-------
APPENDIX D
Capacity Analysis for Second Third Promulgated Wastes
-------
APPENDIX D
The tables in this appendix present the results of the analysis of
required capacity for each alternative technology on a waste code-by-
waste code basis. The tables show the amount of required treatment
capacity for the Second Third promulgated waste codes. The tables also
total the amount of required capacity for each technology.
The original TSDR Survey data were sorted by waste code, waste
description code, and type of alternative treatment required to generate
these tables. Computer printouts showing the original TSDR Survey data
for the Second Third promulgated wastes are contained in Appendix C. The
data were then combined and summarized to create the technology-specific
capacity analysis tables for the Second Third promulgated wastes
contained in Section 2 of this document.
D-l
-------
5710s/l
APPENDIX 0
Capacity Analysis by Technology per Waste Group/Code for
Second Third Promulgated Wastes
Technology: Combustion of liquids
Waste code
F010
F024
K010
K011
K013
P039
P089
P094
U069
U087
U190
U221
U223
Totals
Required capacity
Non-deepwe I 1
volume
(gallons/year)
32.400
9,360
0
49,920
1.920
295
26.880
1,200
29
0
0
0
59.041
181.045
1988
Oeepwell
volume
(gallons/year)
0
0
5.000.000
173,379,980
173,379.980
0
0
0
0
960
9.853
26,824,080
0
378,594,853
Source: TSDR Survey and EPA Office of Drinking Water's Hazardous Waste Injection Well Data Base.
-------
5710S/2
APPENDIX D (continued)
Second Third Promulgated Wastes
Technology: Combustion of sludges/solids
Waste code
F008
FOZ4
K009
K010
K011
K013
ICO 14
K027
K093
K094
K113
K115
P071
P089
U028
U190
U221
Totals
Required capacity
Non-deepwe 1 1
volume
(gallons/year)
17.400
62.880
1.440
1,440
144.359
144,359
16.000
7.486,824
36,480
36.480
82,080
161,760
25,896
480
480
75.120
305.784
8.599,262
1988
Deepwell
volime
(gallons/year)
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
Source: TSDR Survey.
D-3
-------
5710s/3
APPENDIX D (continued)
Second Third Promulgated Wastes
Technology: Stabilization of incinerator ash
Waste code
Required capacity 1988
Non-deepwell
volume
(gallons/year)
Deepwell
volume
(gallons/year)
F008
F010
F024
K011
3.216
9,444
8.062
120
Totals
20,842
Source: TSDR Survey.
D-4
-------
5710S/4
APPENDIX D (continued)
Second Third Promulgated Wastes
Technology: Stabilization of scrubber water treatment sludge
Required capacity 1988
Waste code
Non-deepwell
volume
(gallons/year)
Deepwell
volume
(gallons/year)
F008
F010
F024
icon
174
780
723
6
Totals
1.683
Source: TSDR Survey.
0-5
-------
5710S/5
APPENDIX D (continued)
Second Third Promulgated Wastes
Technology: Alkaline chlonnation
Waste code
F007
F008
F009
F010
F011
F01Z
P029
P030
P063
P069
P098
P106
Totals
Required capacity
Non-dee pwe 11
volume
(gallons/year)
543,769
1,032.571
45,251
45.600
82,868
63,620
0
21,382
4,800
240
308
3.782
1,834.191
1988
Oeepwell
volume
(gallons/year)
126.183,360
15,840
42.480
0
0
0
1,512
22,552
16.900
0
2.952
0
126.285.596
Source: TSDR Survey.
D-o
-------
5710S/6
APPENDIX D (continued)
Second Third Promulgated Wastes
Technology: Chromium reduction and chemical precipitation
Waste code
Required capacity 1988
Non-deepwe11
volume
(gallons/year)
Deepwell
volume
(gallons/year)
F007
F009
113.040
6.480
Totals
119.520
Source: TSDR Survey.
D-7
-------
5710S/7
APPENDIX 0 (continued)
Second Third Promulgated Wastes
Technology: Steam stripping and/or biological treatment
Waste code
Required capacity 1988
Non-deepwe11
volume
(gallons/year)
Deepwell
volume
(gallons/year)
K009
79.000.000
D-8
Totals
79,000.000
Source: TSOR Survey.
-------
5710S/8
APPENDIX D (continued)
Second Third Promulgated Wastes
Technology: Biological treatment
Waste code
Required capacity 1988
Non-deepwell
volume
(gallons/year)
Deepwell
volume
(gallons/year)
P071
P089
1,920
1.200
Totals
3,120
Source: TSDR Survey.
D-9
-------
5710S/9
APPENDIX D (continued)
Second Third Promulgated Wastes
Technology: Stabilization of wastewater treatment sludge
Waste code
Required capacity 1988
Non-deepwe11
volume
(gallons/year)
Oeepwell
volume
(gallons/year)
F007
F008
F009
F010
F011
F012
446.338
999,070
5.147
45.144
45.517
61.338
1,263.905
3.922
489
0
0
0
Totals
1.602.554
1,268.316
Source: TSDR Survey.
D-10
-------
5710S/10
APPENDIX D (continued)
Second Third Promulgated Wastes
Technology: Stabilization
Required capacity
Non-deepwell
volume
Waste code (gallons/year)
F007 242,018
F008 242.018
F009 266,978
F011 3.788
Totals 754.802
1988
Deepwell
volume
(gallons/year)
0
0
0
0
0
Source: TSDR Survey.
D-ll
-------
5710S/11
APPENDIX 0 (continued)
Second Third Promulgated Wastes
Technology: Carbon adsorption or direct combustion of wastewaters
Required capacity 1988
Non-deepwe11 Deepwe11
volume volume
Waste code (gallons/year) (gallons/year)
U223 0 9.853
Totals 0 9,853
Source: EPA Office of Drinking Water's Hazardous Waste Injection Well Data Base.
D-12
-------
APPENDIX E
Waste Volume and Characterization Data
for Underground Injected K009 and K010 Waste
Used to Support the Second Third Final Rule
-------
APPENDIX E
The purpose of this appendix is to document the data used to
determine the volume and characteristics of underground injected K009 and
K010 wastes for the Second Third wastes final rule.
For the proposed rule, the TSDR Survey data base was used to estimate
the volume and characteristics of K009 and K010 wastes. The TSDR Survey
identified only one facility land disposing K009 and K010 wastes. This
facility, the Hoechst Celanese Chemical Group in Bay City, Texas,
reported underground injecting approximately 108 million gallons of mixed
K009 and K010 described as an "aqueous waste with low other toxic
organics." Based on this data, the waste stream was determined to be a
wastewater and a national capacity variance was proposed.
Since publication of the proposed rule, however, EPA's Office of
Drinking Water (ODW) has determined, based on a personal communication
between Mr. Eric Callisto of ODW and a Hoechst Celanese facility
representative, that the actual volume of K009 generated and underground
injected is approximately 79 million gallons per year and the volume of
K010 generated and injected is approximately 5 million gallons per year.
In addition, based on analytical data supplied by the facility (included
as Attachment 1), ODW has determined that the K009 stream is a wastewater
as generated and the K010 stream is a nonwastewater as generated.
Attachment 1 also includes a letter from ODW to the facility informing
them of ODW's decision regarding the physical/chemical form of these
wastes.
E-l
-------
Attachment E-l
K009 and K010 Data
E-2
-------
1
\ UNITED STATES ENVIRONMENTAL PROTECTION AGENCY
o
OFFICE OF
WATER
. WASHINGTON. D.C. 20460
<•*
APR I 8 1989
I.O. Coleman, Jr.
Hoechst Celanese Chemical Group
P.O. Box 509
Bay City, TX 77414
Dear Mr. Colemar.:
Recently, a member of rny staff discussed with Glenn
McCarthy of your staff the classification of certain
hazardous wastes that are deep-well injected at the Hoechst
Celanese Bay City, Texas, facility.
The issue, raised by the Environmental Protection
Agency's proposed Land Disposal Restrictions for Second Third
Scheduled Wastes (54 FR 1056), concerns the K009 and K010
waste codes. In that publication, the Agency requested
additional data on the volumes, composition, and
characteristics of any of these wastes that are underground
injected.
The comments submitted by Hoechst Celanese during the
public comment period, and the data provided on April 10,
1989 (attached), have been evaluated by the Office of
Drinking Water and the Waste Treatment Branch of the Office
of Solid Waste. The data indicate that the K010 tower
sidestream is a nonwastewater, as generated. It also
indicates that the K009 tower residue is a wastewater, as
generated.
If you have any questions on this determination, please
call Bruce Kobelski, Hazardous Waste Injection Section,
Underground Injection Control Branch, at (202) 382-5508.
Sincerely,
Francoise M. Brasier, Chief
Underground Injection Control
Branch
Office of Drinking Water
Attachment
E-3
-------
Hoechst Celanese Chemical Group'ZInc
Bay City, Texas Plant
' firR 10 '89 iu:56 HOESCHT CELPNESE
Date: April 10, 1989
*Vi '
To: Eric Callisto, EPA, Office of Drinking Water
Fro*: Glenn McCarthy, Hoechst Celanese Chemical Group, Bay City, Texaa
Thank you!
i' or 'non-wastewaters'.
(FAX number is (409) 245-4871, extenaion 4086)
Parameter
Total Organic Carbon (TOG)
Total Suspended Solids (TSS)
K-010
TOWEH SIDESTREAM
BCP Analysia
Nov., 1988
23,500
24
SPL Analysis
Nov., 1988
23,500
9
Bg/1
CORE Labs
Feb., 1989
36,830
46
Total Organic Carbon (TOC)
Total Suspended Solida (TSS)
K-009
TOWEB RESIDUE -
fflg/1 mg/l
BCP Analysia SPL Analysis
Nov., 1988 Nov., 1988
og/1
COEE Labs
Feb., 1989
5,500
28
5,560
14
5,490
15
E-4
-------
APPENDIX F
Capacity Analysis for Contaminated Soil Wastes
-------
APPENDIX F
The tables in this appendix present the results of the analysis of
required capacity for each alternative technology for contaminated
soils. The tables show the amount of required capacity for each
technology.
To generate these tables, the original TSDR Survey data were sorted
by waste code, waste description code (i.e., those described as soils),
and type of alternative treatment required. Computer printouts showing
the original TSDR Survey data for the Second Third promulgated wastes are
contained in Appendix C. The data were then combined and summarized to
create the technology-specific capacity analysis tables for contaminated
soils contained in Section 2 of this document.
F-l
-------
APPENDIX F
The tables in this appendix present the results of the analysis of
required capacity for each alternative technology for contaminated
soils. The tables show the amount of required capacity for each
technology.
To generate these tables, the original TSDR Survey data were sorted
by waste code, waste description code (i.e., those described as soils),
and type of alternative treatment required. Computer printouts showing
It—-
the original TSDR Survey data for Second Third promulgated wastes are
A.
contained in Appendix C. The data were then combined and summarized to
create the technology-specific capacity analysis tables for contaminated
soils contained in Section 2 of this document.
F-i
-------
5710s/12
APPENDIX F
Capacity Analysis by Technology per
Waste Group/Code for Contaminated Soil Wastes
Technology: Alkaline chlorination
Required capacity 1988
So Ivents 0
First Third promulgated wastes 0
HOCs (Soft Hanrner First Third and
non-First Third) 0
Second Third promulgated wastes
F007 764,769
F008 596.635
F009 342.018
F011 3,788
P029 240
P030 7,350
P063 15,360
P106 480
Total 1,630,640
Source: TSDR Survey.
F-2
-------
5710S/13
APPENDIX F (Continued)
Technology: Stabilization of wastewater treatment sludge from treatment
of soils
Required capacity 1988
Solvents 0
First Third promulgated wastes 0
HOCs (Soft Hammer First Third and
non-First Third) 0
Second Third promulgated wastes
F007 757.121
F008 590,669
F009 239,598
Full 3.750
Total 1,591,138
Source: TSOR Survey.
F-3
-------
5710s/14
APPENDIX F (Continued)
Technology: Combustion of soils
Required capacity 1988
Solvents 25.736.413
First Third promulgated wastes 11,699.109
HOCs (Soft Hanmer First Third and
non-First Third) 4,174.281
Second Third promulgated wastes
F010 480
KOll 120
K013 120
IU13 240
P044 1,680
P071 46.980
P089 720
P094 43,800
U028 386,160
U069 1,440
U190 11,550
U221 97,200
U223 6.000
Total 42.206,293
Source: TSDR Survey.
F-4
-------
5710s/15
APPENDIX F (Continued)
Technology: Stabilization of incinerator ash from the combustion of soils
Required capacity 1988
Solvents 9,736,000
First Third promulgated wastes 11,459,929
HOCs (Soft Harnner First Third and
non-First Third) 0
Second Third promulgated wastes
F010 475
Total 21,196.404
Source: TSDR Survey.
F-5
-------
5710s/16
APPENDIX F (Continued)
Technology: Stabilization of scrubber water treatment sludge from the
combustion of soils
Required capacity 1988
Solvents 99,689
First Third promulgated wastes 116.087
HOCs (Soft Hanmer First Third and
non-First Third) 0
Second Third promulgated wastes
F010 5
TotaJ 815,781
Source: TSDR Survey.
F-b
-------
APPENDIX G
Alternative Treatment/Recovery
Technology Groups
-------
5695s
APPENDIX G
Alternative Treatment/Recovery Technologies (AT/RT)
for Each Waste Group
TRD
group
1
2
3
4
5
6
7
8
9
10
11
12
13
14
15
16
17
18
19
20
21
22
23
24
25
26
27
28
29
30
31
32
33
34
35
36
37
38
39
40
41
42
43
AT/RT codes
1
1.2
lb,2b
la,2a,3,4
5.21.22
7a.41a
lb,2b.8
9.10
4.11,lb,2b
12.13.49
14.13.50
15
16.10
17
18
19
20
10
5.21,22.3,4
7
23,5.21.22,8
7,12.13.49
5.22,24,25
26.la.2a
26,lb,2b
26. la. 2a, 3, 4
27.7a.41a
28
29
30,31
32.17
34,lb,2b
lb.2b.3,4,ll
10.35
38
lb.2b.5.21,22
la
Ib
la,2a
5.21.22.24,6
52
6.21,22
44
G-l
-------
5695s
APPENDIX G (continued)
TRD
group
44
45
46
47
48
49
50
51
52
53
54
55
56
57
58
59
60
61
62
63 '
64
65
66
67
68
69
70
71
72
73
73A
74
75
77
78
79
81
82
83
84
85
86
87
88
89
90
AT/RT codes
7b.41b
36,40
5.6,21.22
6
4Z.43
5,21,22,67
34.1b,2b
45
46
47.48
39
26.1.2
51
53
la. 2a. 21. 22
56.41
54
55
56a.41a
56b.41b
56c.41c
7,41
14.50
57
58
62
63.64
10.16,30.31
13
59,60
65,66
59,60,61
48,59
7b,36.41b,43
13.68
36.42.43
21.22,70
69
7a
70
1.71,21,22
6, 72, 73
74
75
76
77
G-2
-------
5695s
APPENDIX 6 (continued)
TRD
group AT/RT codes
91 78
92 79
93 80
94 81
95 82
96 83
97 84
98 85
99 86
100 87
101 88
102 89,75
103 90
104 lc
105 91
106 21,22
(i-3
-------
APPENDIX H
Alternative Treatment/Recovery Technologies
-------
5695s
APPENDIX H
Alternative Treatment/Recovery Technologies
Alternative
Treatment/Recovery
Technology Codes
Description
1
la
Ib
Ic
2
2a
2b
3
4
5
6
7
7a
7b
8
9
10
11
1Z
13
14
15
Incineration of solids
Incineration of sludges
Incineration of liquids
Incineration of gases
Reuse as fuel of solids
Reuse as fuel of sludges
Reuse as fuel of liquids
Solvent extraction
Fractionation or batch still distillation
Carbon adsorption
Biological treatment
Incineration of solids followed by
stabilization of the ash and chromium
reduction followed by metals precipitation
of scrubber water with stabilization of
treatment sludge
Incineration of sludges followed by
stabilization of the ash and chromium
reduction followed by metals precipitation
of scrubber water with stabilization of
treatment sludge
Incineration of liquids followed by
stabilization of the ash and chromium
reduction followed by metals precipitation
of scrubber water with stabilization of
treatment sludge
Solvent extraction followed by steam
stripping and carbon adsorption
Retorting followed by stabilization
of the ash
Cement-based or pozzolanic stabilization
Thin film evaporation
Cyanide oxidation followed by chemical
precipitation, sludge dewatering, and
stabilization of the sludge (also 49)
Wet air oxidation followed by carbon
adsorption, chemical precipitation, sludge
dewatering, and stabilization of the sludge
Slurrying followed by cyanide oxidation,
chemical precipitation, sludge dewatering,
and stabilization of the sludge
Chemical precipitation, sludge dewatering,
and stabilization of the sludge
H-l
-------
5695s
APPENDIX H (continued)
Alternative
Treatment/Recovery
Technology Codes
Description
16
17
18
19
20
21
22
23
24
25
26
27
28
29
30
31
32
33
34
35
Slurrying followed by chemical precipitation,
sludge dewatering, and stabilization of the
sludge
Chrome reduction followed by chemical
precipitation, sludge dewatering, and
stabilization
Slurrying followed by chrome reduction,
chemical precipitation, sludge dewatering,
and stabilization
Cyanide oxidation
Slurrying followed by cyanide oxidation
Wet air oxidation followed by carbon adsorption
Wet air oxidation followed by biological
treatment
Solvent extraction followed by steam stripping
Steam or air stripping followed by carbon
adsorption
Fractional ion, batch still distillation, or
solvent extraction followed by incineration
of the organic stream
Rotary kiln or fluidized bed incineration
Rotary kiln or fluidized bed incineration of
sludges followed by stabilization of the ash
and metals precipitation of scrubber water
with stabilization of treatment sludge
Chlorination followed by vacuum filtration,
followed by sulfide precipitation,
filtration, and sludge dewatering of the
filtrate from the vacuum filter
Solvent extraction followed by incineration
or reuse as fuel of the extract and steam
stripping and carbon adsorption of the
wastewater
Secondary smelting
Secondary smelting followed by stabilization
of the slag
Chromium reduction followed by chemical
precipitation and vacuum filtration
Chromium reduction followed by chemical
precipitation and sludge dewatering (17)
Liquid injection incineration or reuse as fuel
Incineration followed by dissolving of the ash,
sulfide precipitation, sludge dewatering,
and stabilization
H-2
-------
5695s
APPENDIX H (continued)
Alternative
Treatment/Recovery
Technology Codes
Description
36
37
38
39
40
41
41a
41b
42
43
44
45
46
47
48
49
Carbon adsorption followed by chromium
reduction, chemical precipitation, sludge
dewatering, and stabilization
Solids blending
Neutralization
Electrochemical cyanide oxidation followed by
alkaline chlorination, chemical
precipitation, sludge dewatering, and
stabilization
Wet air oxidation, followed by carbon
adsorption, chromium reduction, chemical
precipitation, sludge dewatering, and
stabilization (see 43)
Reuse as fuel of solids followed by stabiliza-
tion of the ash from boilers and process
heaters
Reuse as fuel of sludges followed by stabiliza-
tion of the ash from boilers and process
heaters
Reuse as fuel of liquids followed by stabiliza-
tion of the ash from boilers and process
heaters
Stripping followed by carbon adsorption,
chromium reduction, chemical precipitation,
sludge dewatering, and stabilization
Wet air oxidation followed by carbon adsorption,
chromium reduction, chemical precipitation,
sludge dewatering, and stabilization
Steam stripping followed by chemical
precipitation, sludge dewatering, and
stabilization
Sulfide precipitation followed by sludge
dewatering and stabilization
Slurrying followed by sulfide precipitation,
sludge dewatering, and stabilization
Cyanide oxidation followed by sulfide
precipitation, sludge dewatering, and
stabilization
Wet air oxidation, followed by carbon
adsorption, sulfide precipitation, sludge
dewatering, and stabilization
Cyanide oxidation followed by chemical
precipitation, sludge dewatering, and
stabilization
H-3
-------
5695s
APPENDIX H (continued)
Alternative
Treatment/Recovery
Technology Codes
Description
50
51
53
55
56
56a
56b
56c
58
59
60
61
Slurrying followed by cyanide oxidation,
chemical precipitation, sludge dewatering,
and stabilization
The waste already meets BOAT treatment
standard
Lab pack waste
Total recycle of K069
Incineration of solids followed by
stabilization of the ash and chemical
precipitation of the scrubber water followed
by sludge dewatering and stabilization
Incineration of sludges followed by
stabilization of the ash and chemical
precipitation of the scrubber water followed
by sludge dewatering and stabilization
Incineration of liquids followed by
stabilization of the ash and chemical
precipitation of the scrubber water followed
by sludge dewatering and stabilization
Incineration of gases followed by
stabilization of the ash and chemical
precipitation of the scrubber water followed
by sludge dewatering and stabilization
Sludge dewatering followed by incineration
of the solids with stabilization of the ash.
Chromium reduction and chemical precipitation
of the scrubber water followed by sludge
dewatering and stabilization and oil skimning
followed by chromium reduction, chemical
precipitation, and sludge dewatering and
stabilization, of the liquid effluent from
the original dewatering
Carbon adsorption followed by sulfide
precipitation, sludge dewatering, and
stabilization
Biological treatment followed by sulfide
precipitation, sludge dewatering, and
stabilization
Incineration of liquids followed by
stabilization of the ash and chromium
reduction, sulfide precipitation of the
scrubber water followed by sludge dewatering
and stabilization
H-4
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5695s
APPENDIX H (continued)
Alternative
Treatment/Recovery
Technology Codes
Description
62
63
64
65
66
67
68
69
70
71
72
73
74
75
76
77
78
79
80
Slurrying followed by general oxidation, sulfide
precipitation, sludge dewatering, and
stabilization
Oil skinning followed by incineration of the
sludge with stabilization of the ash.
Chromium reduction, chemical precipitation of
the scrubber water followed by sludge
dewatering and stabilization, and chromium
reduction followed by chemical precipitation,
sludge dewatering, and stabilization of the
liquid effluent.
Oil skinning followed by chromium reduction,
chemical precipitation, sludge dewatering,
and stabilization of the liquid effluent.
Reuse as fuel of the sludges followed by
stabilization of the ash from boilers and
process heaters.
Cyanide oxidation followed by chromium
reduction, chemical precipitation, sludge
dewatering, and stabilization
Wet air oxidation followed by chromium
reduction, chemical precipitation, sludge
dewatering, and stabilization
General oxidation with hydrogen peroxide or
potassium permanganate
Carbon adsorption followed by chemical
precipitation, sludge dewatering, and
stabilization
Steam stripping followed by chromium reduction,
chemical precipitation, sludge dewatering,
and stabilization
Nixed RCRA/radioactive wastes
Thermal regeneration of carbon
Steam stripping
Steam stripping followed by biological treatment
Slurrying, chrome reduction, caustic ppt,
solidification of sludge, wastewater ppt with
ferrous salt, vitrification of this sludge
Vitrification
Recycle
Drum rinsing
Slurrying, general oxidation
Controlled incineration
Controlled reaction
H-5
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5695s
APPENDIX H (continued)
Alternative
Treatment/Recovery
Technology Codes
Description
81
82
83
84
85
86
87
88
89
90
91
Neutralization with caustic soda followed by
carbon adsorption
Chrome reduction, sulfide ppt, filtration, and
stabilization of the sludge
Neutralization with ferrous salt
Slurrying, chrome reduction, sulfide ppt,
filtration, and stabilization
Carbon adsorption, chrome reduction, sulfide
ppt, filtration, and stabilization of sludge
Neutralization followed by settling, carbon
adsorption of liquid phase
Precipitation using iron salts
Incineration of solids, stabilization of ash,
sulfide salt and ferrous salt ppt, sludge
dewatering, and stabilization/vitrification
of sludge from scrubber water
Incineration of liquids, stabilization of ash,
ferrous salt ppt of scrubber water,
stabilization/vitrification of sludge (see
also 75)
Chrome reduction, chemical precipitation,
solidification of resulting sludge; further
treatment of resulting wastewater using ppt
with iron salts, sulfide precipitation,
vitrification of resulting sludge
Incineration of liquids, stabilization of ash,
sulfide salt and ferrous salt ppt of scrubber
water, sludge dewatering and stabilization/
vitrification of sludges
H-6
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U.S. Environment?! Protection Agency
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