-------
ANALYTICAL DATA FOR USED OIL SAMPLES
Flash Point CD
Mecals
Aluminum
Arsenic
Barium
Beryllium
Cadmium
Chromium
Cobalt
Copper
Iron
Lead
Magnesium
Manganese
Molybdenum
Nickel
Selenium
Silicon
Silver
Sodium
Tin
Titanium
Vanadium
Zinc
Volatile Organics
Dichlorodifluoromethane
Trichlorofluoromethane
Tricolorotrifluoroethane
1,1,1-Trichloroethane
Trichlgroethylene
Tetrachloroethylene
Phenol
Benzene
Toluene
Ethyl Benzene
Xylenes
Methylene Chloride
PNAs
Naphthalene
Penanthrene/Anthracene
Pyrene
Ber.zo (a) anthracene
Benzo(a)pyrene
Sample Number*!
833(240)834(275)835(276)836(278)837(279)838(331) 839(332)
150
>200 >200
<1
<5
90
<0.2
0.56
<0.5
<0.5
9.8
6.7
16
25
2.5
<1
590
<5
7.8
<0.21
<0.5
2.2
0.68
1,4
130
44
1.6
0.42
<1
770
<5
14
<0.2
<0.5
1.5
<0.5
4.0
270
330
2.3
0.4
<1
760
<5
14
<0.2
<0.5
1.5
<0.5
3.6
220
290
1.3
<0.2
<1
910
<5
24
<0.2
<0.5
2.1
<0.5
6.0
170
220
3.6
0.53
<1
16
<5
120
<0.2
0.7
10
0.8
20
110
59
16
2.0
40
410
<5
5.0
<0.2
<0.5
2.0
<0.5
2.0
240
7.3
6.2
3.0
1.1
2.3 5.7 2.4 1.7
3.3 5.9
3.2
<0.2 <0.2 <0.2 <0.2 <0.2 <0.2 <0.2
200 3.7 2.3 1.9 6.0 120 30
<14 <16 <15 <16 <4
<14 <16 <15 <16 <4
<14 <16 <15 <16 <4
<14 <16 <15 <16 <4
<14 <16 <15 <16 <4
<14 <16 <15 <16 <4
540 <16 <15 <16 37
<14 <16 <15 <16 <4
Alkylbenzene (CgH..)
Alkylnaphthalene tc.-lL-)
Phosphorus
Chlorine, wt X
Sulfur, wt 2
PCBs
350
8.67
0.60
<5
280
0.07
0.49
<5
220
<0.01
0.39
<5
110
<0.01
0.45
<5
91
<0.01
0.06
<5
280
0.06
-
<5
240
0.15
-
<5
* Table A-2 identifies the source of analytical data for each used oil sample. Table A-3 provides codes
for each sample number which describes the specific generating source of used oil and the end-use.
T Numbers in parentheses represent EPA sample numbers for used oil samples obtained as part of their
1983 sampling program.
A-100
-------
TABLE A-l (continued)
ANALYTICAL DATA TOR USED OIL SAMPLES
Sample Number*
840 841 842 843 844 845 846 847
Flash Point (°F) ________
Metals
Aluminum ----____
Arsenic ________
Barium 82 96.2 88 81.3 88.3 89.5 79.4 85
Beryllium ________
Cadmium 2.7 3 5 4.7 4.8 2 4.2 2.7
Chromium 9.8 12 16.3 8 14.5 16.8 12.8 6.3
Cobalt ________
Copper ________
Iron ________
Lead 93.8 257.3 118.3 86 129.7 21.8 183.6 87.5
Magnesium ________
Manganese ________
Molybdenum ________
Nickel ________
Selenium ________
Silicon ________
Silver ________
Sodium ________
Tin ________
Titanium ________
Vanadium ________
Zinc 1,125 965 900 1,100 1,133 1,020 1,166 923
Volatile Organics
Dichlorodifluoromethane ________
Trichlorofluoromethane ________
Trichlorotrifluoroethane ________
1,1,1-Trichloroethane ________
Trichloroethylene ________
Tetrachloroethylene ________
Phenol ________
Benzene - - - - - --
Toluene ________
Ethyl Benzene ________
Xylenes ________
Methylene Chloride - " -
PNAs
naphthalene ________
Penanthrene/Anthracene - - - - - - - -
Pyrene ________
Benzo(a)anthracene ________
Benzo(a)pyrene ________
Alkylbenzene (C H ,) ________
Alkylnaphthalene tC1_H1_) ________
Phosphorus i- i- ________
Chlorine, wtZ ________
Sulfur, wt % ________
PCBs ________
* Table A-2 identifies the source of analytical data for each used oil sample. Table A-3 provides codes
for each sample number which describes the specific generating source of used oil and the end-use.
A-101
0283
-------
TABLE A-l (continued)
ANALYTICAL DATA FOR USED OIL SAMPLES
Sample Number*
86.3
6.5
12.8
87
4.0
11.0
77.5
0.3
5.8
91.5
0.9
9.5
75.0
2.0
11.5
103.1
0.7
8.1
102.3
1.3
7.7
T6.5
0.5
5.0
848 849 850 851 852 853 854 855
Flash Point (°F) ________
Metals
Aluminum ~ ~ * ~ _ *
Arsenic
Barium
Beryllium
Cadmium
Chromium
Cobalt _________
Copper ________
Iron ________
Lead 161.3 77.8 120 85.1 115 95.8 53 69.0
Magnesium ________
Manganese __.-__«_
Molybdenum ________
Nickel ________
Selenium ________
Silicon ________
Silver ________
Sodium ________
Tin ________
Titanium ________
Vanadium ________
Zinc 950 1.160 1,758 906.3 1,050 951.4 936.7 1,125
Volatile Organics
Dichlorodifluorotnethane ________
Trichlorofluoromethane ________
Trichlorotrifluoroethane ________
1,1,1-Trichloroethane ________
Trichloroethylene ________
Tetrachloroethylene -___-__
Phenol ________
Benzene ________
Toluene _----___
Ethyl Benzene __-_---_
Xylenes --- - - - _
Methylene Chloride ________
PNAs
Naphthalene ________
Penantnrene/Anthracene ________
Pyrene ________
Benzo(a)anthracene ________
Benzo(a)pyrene ________
Alkylbenzene (CqH12) ________
Alkylnaphthalene tc,-H ,) -
Phosphorus ^ ________
Chlorine, wtX ________
Sulfur, wtl ________
PCBs ________
* Table A-2 identifies the source of analytical data for each used oil sample. Table A-3 provides codes
for each sample number which describes the specific generating source of used oil and the end-use.
A-102
-------
TABLE A-l (continued)
ANALYTICAL DATA FOR USED OIL SAMPLES
Flash Point (°F)
Metals
Aluminum
Arsenic
Barium
Beryllium
Cadmium
Chromium
Cobalt
Copper
Iron
Lead
Magnesium
Manganese
Molybdenum
Nickel
Selenium
Silicon
Silver
Sodium
Tin
Titanium
Vanadium
Zinc
856
94.8
1.1
7.7
91.3
Sample Number*
857
82.8
0.2
5.8
51.0
858
83.5
1.3
10.0
82.0
859
80.6
0.2
5.8
860
95.6
0.7
6.0
87.3 103.3
861
90.0
1.7
7.7
84.3
862
65.0
3.0
10.0
863
74.8
2.4
7.9
90.0 309.3
1,251 1,522
917.5 1,541 1,157
842 1,050 1,177
Volatile Organics
Dichlorodifluorome thane
Trie hi orofluorome thane
Trichlorotrif luoroethane
1 ,1,1-Trichloroethane
Trichloroethyleixe
Tetrachloroethylene
Phenol
Benzene
Toluene
Ethyl Benzene
Xylenes
Methylene Chloride
PNAs
Naphthalene
Penanthrene /Anthracene
Pyrene
Benzo(a)anthracene
Benzo(a)pyrene
Alkylbenzene (ClL )
Alkylnaphthalen
Phosphorus
Chlorine, wt Z
Sulfur, vt 7.
PCBs
. -,H1-)
* Table A-2 identifies the source of analytical data for each used oil sample. Table A-3 provides codes
for each sample number which describes the specific generating source of used oil and the end-use.
A-103
0285
-------
TABLE A-l (continued)
ANALYTICAL DATA TOR USED OIL SAMPLES
Flash Point (°f)
Metals
Aluminum
Arsenic
Barium
Beryllium
Cadmium
Chromium
Cobalt
Copper
Iron
Lead
Magnesium
Manganese
Molybdenum
Nickel
Selenium
Silicon
Silver
Sodium
Tin
Titanium
Vanadium
Zinc
Volatile Organics
Dithlorodifluoromethane
Trichlorofluoromethane
Trichlorotrifluoroethane
1,1,1-Trichloroethane
Trichloroethylene
Tetrachloroethylene
Phenol
Benzene
Toluene
Ethyl Benzene
Xylenes
Methylene Chloride
PNAs
Naphthalene
Penanthrene/Anthracene
Pyrene
Benzo(a)anthracene
Benzo(a)pyrene
Alkylbenzene (CqH,,)
Alkylnaphthalene tc.,H ,)
Phosphorus
Chlorine, wt Z
Sulfur, wt 2
PCBs
Sample Sunbcr*
864
865
866
867
868
869
870
871
82.5
1.1
8.7
68.4
0.6
12.0
102.5 1,323.3
84.3
0.5
5.0
70.2
76.1
2.0
8.0
56.3
94.3
1.4
6.0
77.4
85.1
1.4
10.4
69.8
1.3
15.3
78.9 133.4
76.0
5.8
97.6
915 1,291
872 1,082.8 901 1,600 1,644
916
* Table A-2 identifies the source of analytical data for each used oil sample. Table A-3 provides codes
for each sample number which describes the specific generating source of used oil and the end-use.
A-104
-------
TABLE A-l (continued)
ANALYTICAL DATA FOR USED OIL SAMPLES
"lash Point (?)
Metals
Aluminum
Arsenic
Barium
Beryllium
Cadmium
Chromium
Cobalt
Copper
Iron
Lead
Magnesium
Manganese
Molybdenum
Nickel
Selenium
Silicon
Silver
Sodium
Tin
Titanium
Vanadium
Zinc
Volatile Organics
);ichlorodifluorome thane
Trichlorofluoromethane
Trichlorotrifluoroethane
1,1,1-Trichloroethane
Trichloroethylene
Tetrachloroethylene
Phenol
Benzene
Toluene
Ethyl Benzene
Xylenes
Methylene Chloride
PSAs
Naphthalene
Penanthrene/Anthracene
Pyrene
Benz o (a) ant hracene
Benzo(a)pyrene
Alkylbenzene (CqH17)
Alkylnaphthalene tc. -1L.)
Phosphorus "
Chlorine, wt %
Sulfur, wt Z
PCBs
Sample Number*
872
873
874
875
876
877
878
879
79.0
0.3
25.3
77.9
1.0
18.6
70.0
0.6
32.6
87.3
0.3
31.0
70.0
0.7
25.0
67.7
0.3
26.7
68.0 30.7
0.9
21.3
1.0
19.3
12.242 18,063 18,500 12.400 20.333 17.8 16,637 17,037
915
980 1,214 1.077 1,050 1.067 1,169 1.112.5
* Table A-2 identifies the source of analytical data for each used oil sample. Table A-3 provides codes
for each sample number which describes the specific generating source of used oil and the end-use.
A-105
0286
-------
TABLE A-l (concinued)
ANALYTICAL DATA FOR USED OIL SAMPLES
Sample Number*
Flash Point (*F)
Metals
Aluminum
Arsenic
Barium
Beryllium
Cadmium
Chromium
Cobalt
Copper
Iron
Lead
Magnesium
Manganese
Molybdenum
Nickel
Selenium
Silicon
Silver
Sodium
Tin
Titanium
Vanadium
Zinc
Volatile Organics
Dichlorodif luorome thane
Tr ichlorof luor ometnane
Trichlorotrif luoroe thane
1,1,1-Trichl or oe thane
Trichloroethylene
Tetrachloroethylene
Phenol
Benzene
Toluene
Ethyl Benzene
Xylenes
Methylene Chloride
880
>147
-
<5
<7
-
<7
<5
-
<5
11
6
-
-
<5
<5
-
-
-
-
-
-
<5
254
-
-
-'
2,300
<100
<100
-
-
-
-
-
-
881
142
-
9
<7
-
< 7
6
18
113
202
-
-
<5
<5
-
-
-
-
-
-
<5
197
-
-
-
9,200
<100
<100
-
-
.
-
-
-
882
M47
-
<5
10
-
<7
14
-
43
48
16
-
-
<5
<5
-
-
-
-
-
-
<5
168
-
-
-
600
<100
<100
-
-
-
-
-
-
883
>147
-
<5
18
-
147
-
18
31
-
<7
9
_
38
184
1,000
-
-
<6
<5
-
-
-
-
-
-
<5
952
-
-
-
4,700
<100
300
-
-
-
-
-
-
885
133
_
13
19
-
9
9
_
38
148
507
-
-
<6
<5
-
_
_
-
_
_
<5
380
_
_
_
10,000
.4.200
3,000
_
-
_
-
-
-
886
142
_
<5
90
_
<5
52
»
69
783
725
-
-
19
<5
-
.
_
-
_
_
19
597
_
_
_
2,700
1,900
1,900
v
_
_
-
-
-
887
>147
_
22
10
_
<5
<5
»
30
107
1,240
-
.
<6
<5
_
_
_
_
_
<5
300
_
_
_
6,000
1,400
11,000
_
_
_
-
-
-
PNAs
Naphthalene
Penanthrene /Anthracene
Pyrene
Benzo (a) anthracene
Benzo(a)pyrene
Alkylbenzene (Cg
Alkylnaphthalene
Phosphorus
Chlorine, vt Z
Sulfur, vl I
PCBs
0.19 0.99 0.08 3.23 0.36
1.95
<50
0.32 3.26
* Table A-2 identifies the source of analytical data for each used oil sample. Table A-3 provides codes
for each sample number which describes the specific generating source of used oil and the end-use.
A-106
-------
ANALYTICAL DATA FOR USED OIL SAMPLES
Sample Number*
Flash Point CF)
Metals
Aluminum
Arsenic
Barium
Beryllium
Cadmium
Chromium
Cobalt
Copper
Iron
* Lead
Magnesium
Manganese
Molybdenum
Nickel
Selenium
Silicon
Silver
Sodium
Tin
Titanium
Vanadium
Zinc
Volatile Organics
Dichlorodifluorome thane
Trichlorofluoromethane
Trichlorotrifluoroe thane
1,1, 1-Trichloroe thane
Trichloroethylene
Tetrachloroethylene
Phenol
Benzene
Toluene
Ethvl Benzene
Xvlerxes
Methylene Chloride
888
108
-
18
17
-
<5
<5
-
60
102
1,200
-
-
<6
<5
-
-
-
-
-
-
<5
366
-
-
-
5,200
5,700
24,000
-
-
-
-
-
-
889 890
>U7
- -
<5 <5
99 39
-
9 <5
126 31
-
89 16
671 337
915 28
-
-
8 <6
<5 <5
-
-
-
-
-
- -
7 <5
214 50
-
-
- -
30,000
800
4,500
-
-
-
-
-
-
891
>147
-
<5
<9
-
<5
<5
-
<5
5
<5
-
-
<6
<5
-
-
-
-
-
-
<5
<5
-
-
-
<100
<100
<100
-
-
-
-
-
892
)147
-
<5
284
-
<5
37
-
103
613
141
-
-
<6
<5
-
-
-
-
-
-
6
148
-
-
-
900
<100
<100
-
-
-
-
-
-
893 894
>147 >147
- -
<5 <5
42 91
_ ;
<5 <5
<5 7
-
6 6
87 2.570
5 57
-
- -
<6 <6
<5 15
-
-
-
-
-
- -
<5 22
8 224
-
-
- -
200
-
- -
-
-
-
-
-
895
>147
-
26
40
-
<10
8
-
53
173
815
-
-
5
<5
-
-
-
-
-
-
<5
962
-
-
-
<100
<100
<100
-
-
-
-
-
-
PSAs
Naphthalene __-__-__
Penanthrene/Anthracene __-__-__
Pyrene ________
Benzo(a)anthracene ________
Benzo(a)pyrene ________
Alkylbenzene (C.H..) __-_-___
Alkylnaphthalene tc.-H,,) __----_-
Phosphorus --------
Chlorine, wt % *-72 1.22 0.35 <0.01 0.34 0.26 0.29 0.04
Sulfur, wt% __-__-__
PCBs <10 <50 - <1 <50 - <10 <10
* Table A-2 identifies the source of analytical data for each used oil sample. Table A-3 provides codes
for each sample number which describes the specific generating source of used oil and the end-use.
A-107
0287
-------
TABLE A-l (continued)
ANALYTICAL DATA FOR USED OIL SAMPLES
Sample Number*
896 897
Flash Point (°T> >147 >147
Metals
Aluminum
Arsenic 19 9
Barium 30 40
Beryllium
Cadmium <10 <10
Chromium 25 118
Cobalt
Copper 34 63
Iron 166 282
Lead 636 725
Magnesium
Manganese
Molybdenum <5 6
Nickel <5 <5
Selenium
Silicon
Silver
Sodium
Tin
Titanium
Vanadium <5 <5
Zinc 923 569
Volatile Organics
Dichlorodifluoromethane
Trichlorofluoromethane
Trichlorotrifluoroethane
1.1,1-Trichloroethane 200 <100
Trichloroethylene <100 <100
Tetrachloroethylene 600 20,000
Phenol
Benzene -
Toiuer.e
Ethyl Benzene
Xylenes -
Methylene Chloride
PSAs
Naphthalene -
P enar.Lhrene/Anthracene
Pyrene
Benzo(a)anthracene
Benzo(a)pyrene - -
Alkylber.zene (CQH.,)
Alkylnaphthalene tc. ,H .)
Phosphorus -
Chlorine, wt 7. 0.11 3.69
Sulfur, wt % - -
PCBs <10 <10
* Table A-2 identifies the source of analytical data for each used oil sample. Table A-3 provides codes
for each sample number which describes the specific generating source of used oil and the end-use.
A-108
-------
TABLE A-l (continued)
ANALYTICAL DATA FOR USED OIL SAMPLES
Sample Number*
Flash Point (°F)
Metals
Aluminum
Arsenic
Barium
Beryllium
Cadmium
Chromium
Cobalt
Copper
Iron
Lead
Magnesium
Manganese
Molybdenum
Nickel
Selenium
Silicon
Silver
Sodium
Tin
Titanium
Vanadium
Zinc
Volatile Organics
Dichlorodifluoromethane
Trichlorofluoromethane
Trichlorotrifluoroethane
1,1,1-Trichloroethane
Tn;r.loroethylene
letraenioroethylene
Phenol
Benzene
Toluene
Ethyl Benzene
Xylenes
Metr.vlene Chloride
PNAs
Naphthalene
Penanthrene/Anthracene
Pyrene
Benz o(a)anthracene
B«nzo(a)pyrene
898
>147
<5
<7
<7
9
44
270
39
<5
27
<5
86
<100
<100
<100
899
>147
<5
31
<7
<5
156
11
15
16
<5
36
<100
<100
<100
Alkylbenzene (C.Ii
Alkylnaphthalene
Phosphorus
Chlorine, wt Z
Sulfur, wt X
?CBs
900
>147
<5
82
<7
13
37
221
72
<5
11
901
>147
<5
11
<7
<5
21
232
20
<5
7
<5
566
1,600
200
3,800
<5
54
<100
600
600
902
>147
<5
<7
<7
<5
6
33
11
<5
<5
<5
<5
200
<100
<100
903
>147
<5
10
<7
11
30
316
41
6
33
<5
76
2,400
200
1,300
904
>147
<5
29
<7
10
34
306
30
7
26
<5
183
905
>147
<5
<7
<7
7
46
73
<5
<5
<5
<5
<5
1,600 900
200 <100
7,700 200
1.34
<50
0.05
1.38
<50
0.72
<50
1.20
<50
1.14
<50
1.40 0.61
<50 <10
* Table A-2 identifies the source of analytical data for each used oil sample. Table A-3 provides codes
for each sample number which describes the specific generating source of used oil and Che end-use.
A-109
0288
-------
TABLE A-l (continued)
ANALYTICAL DATA FOR USED OIL SAMPLES
Sample Number*
Flash Point (°F)
Metals
Aluminum
Arsenic
Barium
Beryllium
Cadmium
Chromium
Cobalt
Copper
Iron
Lead
Magnesium
Manganese
Molybdenum
Nickel
Selenium
Silicon
Silver
Sodium
Tin
Ticaniun
Vanadium
Zinc
906
TCT
_
<5
18
-
<7
16
-
6
482
13
-
-
12
21
-
-
-
-
-
'
<5
47
907
-
<5
55
-
<7
91
-
71
1.100
18
-
-
315
47
-
-
-
-
-
-
<5
106
908
>147
-
<5
10
-
<7
12
-
25
392
40
-
-
7
23
-
-
-
-
-
-
<5
116
322
>147
_
<5
38
<7
8
-
16
212
39
-
-
<5
8
-
-
-
-
-
.
<5
249
*
«,
<5
41
-
<7
62
-
55
321
<5
-
-
58
15
-
-
-
-
-
-
<5
34
911
w
<5
33
_
<7
181
_
201
28
<5
-
-
31
13
.
-
-
-
-
_
<5
86
912
^
<5
1.100
_
27
440
_
1,140
12.300
893
-
-
987
1.840
-
_
-
-
_
_
450
8.610
913
<5
116
.
<7
209
_
76
3.250
57
-
-
45
100
_
_
_
_
_
_
19
1.600
Volatile Organics
Dichlorodifluoromethane
Trichloroiluoromethane
Trichlorotrifluoroethane
1,1,1-Trichloroethane
Trichloroethylene
Tetrachloroethylene
Phenol
Benzene
Toluene
Ethyl Benzene
Xylenes
Methylene Chloride
PNAs
Naphthalene
Penanthrene/Anthracene
Pyrene
Benzo(a)anthracene
Benzo(a)pyrene
Alkylbenzene (C-H.,)
Alkylnaphthalene tc.-Hj-)
Phosphorus
200"
400
1,000
5,100
100
400
1,500
400
6.900
<100
<100
<100
<100
<100
<100
500
200
2.100
Chlorine, wt X
Sulfur, wt I
PCBs
0.64 0.29 1.07
-
<50 - <50
1.53 0.09
-
<50 <10
0.10 0.20 0.65
-
<10 - <50
* Table A-2 identifies the source of analytical data for each used oil sample. Table A-3 provides codes
for each sample number which describes the specific generating source of used oil and the end-use.
A-110
-------
TABLE A-l (concinued)
ANALYTICAL DATA FOR USED OIL SAMPLES
Sample Number*
Flash Point (CF)
Metals
Aluminum
Arsenic
Barium
Beryllium
Cadmium
Chromium
Cobalt
Copper
Iron
Lead
Magnesium
Manganese
Molybdenum
Nickel
Selenium
Silicon
Silver
Sodium
Tin
Titanium
Vanadium
Zinc
Volatile Organics
Dichlorodifluoromethane
Trichlorof luorotne thane
Trichlorotrifluoroethane
1,1,1-Trichloroethane
Trichloroethylene
Tetrachloroethylene
Phenol
Toluene
Ethyl Benzene
Xvlenes
Methylene Chloride
PN'As
Napnthaier.e
Penant hrene /Ant hracene
Pyrene
Benzo(a)anthracene
Benzo(a)pyrene
Alkylbenzene (CgH,,)
Alkylnaphthalene ^i2H\2^
Phosphorus
Chlorine, wt %
Sulfur, wt 7.
?C5s
914
>147
<5
547
18
363
237
15,000
1,180
1,490
721
117
8.120
915
>147
<5
205
<7
253
>147
9
552
8
571
149 1,160
1,020 4,930
33 317
96
96
387
528
917
>147
<5
70
<7
31
11
152
30
<5
7
36
588
300
200
1,000
113
3,550
<5
152
1,000
800
300
0.46
0.15
0.20
0.43
918
>147
<5
458
<7
125
66
3,150
64
30
322
919
>147
<5
61
<7
24
<5
307
19
<5
7
384
650
<5
122
<100 <100
<100 1,000
<100 1,000
0.15
1.01
<50
920
>147
<5
12
<7
42
26
<5
18
<5
<5
13
9_21
>147
5
22
<5
10
22
549
118
<6
6
<5
392
1.000
200
3,000
0.13
0.45
* Table A-2 identifies the source of analytical data for each used oil sample. Table A-3 provides codes
for each sample number which describes the specific generating source of used oil and the end-use.
A-lll
0289
-------
TABLE A-l (continued)
ANALYTICAL DATA FOR USED OIL SAMPLES
Sample Dumber*
Flash Point (°F)
Metals
Aluminum
Arsenic
Barium
Beryllium
Cadmium
Chromiun
Cobalt
Copper
Iron
Lead
Magnesium
Manganese
Molybdenum
Nickel
Selenium
Silicon
Silver
Sodium
Tin
Titanium
Vanadium
Zinc
Volatile Organics
Dichlorodifluorome thane
Trichlorof luorotne thane
Tr ichlorotr if luoroe thane
1,1, 1-Trichloroethane
Trichloroethylene
Tetrachloroethylene
Phenol
Benzene
Toluene
Icrr. I Ber.zene
Xylenes
Methylene Chloride
922
>147
-
21
29
-
<5
8
-
20
170
502
-
-
<6
<5
-
-
-
-
-
-
<5
593
-
-
-
200
800
200
-
-
-
-
-
-
923
>147
-
<5
13
-
<5
7
-
42
110
11
-
<6
<5
-
-
-
-
-
-
<5
50
-
-
-
<100
<100
<100
-
-
-
-
-
-
924
>147
-
<5
28
-
<5
11
-
26
597
104
-
-
<6
9
-
-
-
-
-
-
<5
333
-
-
-
800
400
300
_
-
-
-
-
-
925
>147
-
<5
292
-
33
511
100
3.260
114
-
12
48
-
-
-
-
-
-
164
188
-
-
-
<100
<100
<100
_
-
-
-
-
-
926
>147
_
<5
76
_
7
84
_
34
1.080
10
-
-
<6
17
-
-
.
.
.
.
41
51
_
-
-
-
-
-
_
-
_
-
-
-
927
>147
_
<5
79
<5
107
_
363
1.150
163
-
-
7
10
.
-
_
_
_
_
28
203
_
-
_
<100
200
<100
_
_
_
-
-
-
928
>147
_
<2
32
<5
28
_
29
502
<5
-
-
<6
<5
-
-
«
-
_
_
10
34
_
-
_
<100
<100
300
_
_
_
-
-
-
929
>147
^
4
26
<5
<5
_
<5
690
86
-
_
<6
47
_
-
_
_
_
_
<5
368
_
<100
<100
200
_
.
-
-
-
PSAs
Naphthalene
Penanthrene/Anthracene
Pyrer.e
Benzo(a)anthracene
Benzo(a)pyrene
Alkylbenzene (CgH^.)
Alkylnaphtr.slene tc.^H.,)
Phosphorus
Chlorine, wt X
Sulfur, wt %
PCBs
---_-___
" " ^ -f ^
0.26 0.54 0.32 0.08 0.03 0.15 0.08 0.19
---_-___
* Table A-2 identifies the source of analytical data for each used oil sample. Table A-3 provides codes
for each sample number which describes the specific generating source of used oil and the end-use.
A-112
-------
TABLE A-l (continued)
ANALYTICAL DATA FOR USED OIL SAMPLES
Sample Number*
Flash Point (°F)
930
97
931
>147
932
61
933
>U7
934
97
935
>147
936
68
937
>147
Metals
Aluminum
Arsenic
Barium
Beryllium
Cadmium
Chromium
Cobalt
Copper
Iron
Lead
Magnesium
Manganese
Molybdenum
Nickel
Selenium
Silicon
Silver
Sodiun
Tin
Titanium
Vanadium
Zinc
Volatile Organics
Dichlorodifluorome thane
Trichlorofluorome thane
Trichlorotrifluoroethane
1,1, 1-Trichloroethane
Trichloroethylene
Tetrachloroethylene
Phenol
Benzene
Toluene
Ethyl Benzene
Xylenes
Methylene Chloride
PNAs
Naphthalene
Penan threr.e /Anthracene
Pyrene
Benzo (a ) anthracene
Benzo(a)pyrene
6
30
<5
124
264
1,100
240
<6
19
<5
233
<100
<100
200
Alkylbenzene
Alkylnaphthalene
Phosphorus
Chlorine, wt Z
Sulfur, wt "
PCBs
(C-H,0
0)
0.22
<2
75
7
<5
9
425
10
<6
<5
27
39
0.05
4
9
<5
<5
16
572
115
<6
10
<5
136
300
<100
1.500
0.35
<2
26
<5
<5
<6
<5
6
47
<100
<100
<100
0.02
6
31
<5
50
8 86
176 1.030
<5 350
<6
5
7
172
4,400
2.200
4.800
<5
91
<5
25
57
416
21
<6
<5
<5
379
9
106
19
51
74
60
600
500
800
373
518
<5
251
<5
6
105 58
8.330 728
404 35
<6
<5
7
220
<100 4,400
<100 <100
900 <100
L.32
<50
0.21
0.65
<50
* Table A-2 identifies the source of analytical data for each used oil sample. Table A-3 provides codes
for each sample number which describes the specific generating source of used oil and the end-use.
A-113
0290
-------
TABLE A-l ^continued;
ANALYTICAL DATA FOR USED OIL SAMPLES
Sample Number*
Flash Point (°F)
Metals
Aluminum
Arsenic
Barium
Beryllium
Cadmium
Chromium
Cobalt
Copper
Iron
Lead
Magnesium
Manganese
Molybdenum
Nickel
Selenium
Silicon
Silver
Sodium
Tin
Titanium
Vanadium
Zinc
Volatile Organics
Dichlorodifluoromethane
Trichlorofluoromethane
Trichlorotrif luoroe thane
1,1,1-Trichloroethane
Trichloroethylene
Tetrachloroethylene
Phenol
Benzene
Toluene
Ethvl Benzene
Xyier.es
Methylene Chloride
938
>147
-
<5
622
-
<5
42
-
167
1,220
52
-
-
<6
<5
-
-
-
-
-
-
27
252
-
-
-
5.400
<100
<100
-
-
-
-
-
-
939
>147
-
<5
718
-
<5
12
-
52
1.030
26
-
-
<6
<5
-
-
-
-
-
-
14
235
-
-
-
300
<100
<100
-
-
-
-
-
-
940
>147
-
<5
66
-
<5
<5
-
17
96
<5
-
-
<6
<5
-
-
-
-
-
-
<5
17
-
-
-
-
-
-
-
-
-
-
-
941
>147
-
<5
200
-
<5
8
-
75
252
24
-
-
<6
<5
-
-
-
-
-
-
<5
99
-
-
1.400
<100
<100
-
-
-
-
-
942
>147
-
<5
168
-
<5
10
-
6
201
10
-
-
<6
<5
-
-
-
-
-
-
<5
52
-
-
-
5,500
200
<100
-
-
-
-
943
>147
-
<5
74
-
<5
<5
-
17
114
<5
-
-
<6
<5
-
-
-
-
-
-
<5
9
-
-
-
-
-
-
~
-
944
>147
-
<5
159
- "
<5
12
-
159
374
32
-
-
<6
<5
-
-
-
-
-
-
11
187
-
-
<100
<100
<100
~
~
-
945
>147
-
<5
212
-
<5
15
-
124
434
25
-
-
<6
<5
-
-
-
-
-
-
<5
170
-
-
-
3,800
<100
<100
*
""
*
PKAs
Naphthalene
Penanthrene/Anthracene
Pyrene
Benzo(a)anthracene
Benzo(a)pyrene
Alkylbenzene (CgHj_)
Alkylnaphthalene TC,,H1,)
Phosphorus
Chlorine, wt Z
Sulfur, wt Z
PCBs
0.50
-
<50
0.10 0.17
-
<20
0.50
-
<50
1.05 0.19
- *
<50
0.04
<5
0.81
*
<50
* Table A-2 identifies Che source of analytical data for each used oil sample. Table A-3 provides codes
for each sample number which describes the specific generating source of used oil and the end-use.
A-114
-------
TABLE A-l (continued)
ANALYTICAL DATA FOR USED OIL SAMPLES
Sample Number*
946 947
Flash Point (8F) -
Metals
Aluminum - -
Arsenic <5 <5
Barium 524 171
Beryllium
Cadmium <5 <5
Chromium 36 11
Cobalt
Copper 210 84
Iron 2.990 338
Lead 44 26
Magnesium
Manganese
Molybdenum
Phosphorus
Chlorine, wt X 0.27 0.34
Sulfur, wt % -
PCBs - <50
* Table A-2 identifies the source of analytical data for each used oil sample. Table A-3 provides codes
for each sample number which describes the specific generating source of used oil and the end-use.
A-115
0291
-------
TABLE A-l (.continues,)
ANALYTICAL DATA FOR USED OIL SAMPLES
Sample Number*
Flash Point (°F)
Metals
Aluminum
Arsenic
Barium
Beryllium
Cadmium
Chromium
Cobalt
Copper
Iron
Lead
Magnesium
Manganese
Molybdenum
Nickel
Selenium
Silicon
Silver
Sodium
Tin
Titanium
Vanadium
Zinc
Volatile Organics
Dichlorodif luoromethane
Trichlorof luoromethane
Tr ichlorotr if luoroe thane
1,1, 1-Trichloroethane
Trichloroethylene
Tetrachloroethylene
Phenol
Benzene
Toluene
Et-.yl 3er.zeT\e
Xylenes
Methylene Chloride
948
129
-
<5
122
-
<7
42
-
82
2.560
1,160
-
-
<5
20
-
-
-
-
-
-
26
1,160
-
-
-
5,000
200
600
-
-
-
-
-
- ,
9_49
117
-
12
16
-
<7
72
-
181
1.260
321
-
-
<5
«5
-
-
-
-
-
-
6
83
-
-
-
200
<100
1,100
-
-
-
-
-
-
950
>147
-
<5
217
-
<7
32
-
21
1,580
1,760
-
-
12
14
-
-
-
-
-
-
37
1.680
-
-
-
400
<100
200
-
-
-
-
-
-
951
>147
-
<5
249
-
<7
45
-
172
2,630
191
-
-
<5
13
-
-
-
-
-
-
29
255
-
-
-
<100
<100
<100
-
-
-
-
-
-
952
>147
-
147
.
8
9
-
<7
332
_
612
2,040
106
-
-
7
17
.
.
-
-
-
-
<5
122
_
-
.
<100
<100
<100
-
-
_
-
-
-
954
>147
_
6
<7
-
<7
47
_
448
1,490
102
-
-
<5
10
_
.
_
-
-
_
<5
56
_
-
-
<100
<100
<100
-
-
_
.
-
-
955
>147
_
16
48
.
<7
241
_
550
4,690
595
-
-
9
32
_
_
_
-
_
.
9
512
_
-
-
<100
<100
<100
_
-
_
-
-
-
PNAs
Naphthalene
Penan threne/Anthracene
Pyrer.e
Benzo(a) anthracene
Benzo(a)pyrene
Alkylbenzene (C.H..)
Alkylnaphthalene tC.,)
Phosphorus
Chlorine, wt Z
Sulfur, wt 2
FCBs
_
0.56 0.40 0.39 0.10
_ _ _ _
<10 <10 <5 <5
-
0.07
-
32
-
<0.01
-
11
-
<0.01
-
7
-
0.04
-
'5
* Table A-2 identifies the source of analytical data for each used oil sample. Table A-3 provides codes
for each sample number which describes the specific generating source of used oil and the end-use.
A-116
-------
ANALYTICAL DATA FOR USET) OIL SAMPLES
Sample Number*
Flash Point (cf)
Mecals
Aluminum
Arsenic
Barium
Beryllium
Cadnuun
Chromium
Cobalt
Copper
Iron
Lead
Magnesium
Manganese
Molybdenum
Nickel
Selenium
Silicon
Silver
Sodium
Tin
Titaniun
Vanadium
Zinc
Volatile Organics
Dichlorodif luor one thane
Trichlorofluoromethane
Trichl orotr if luoroe thane
1,1, 1-Irichloroethane
Trichloroethylene
Tetrachloroethylene
Phenol
Benzene
Toluene
Ethvl Benzene
Xyler.e;
Methylene Chloride
956
>147
_
10
1.070
-
<7
87
-
600
8,570
388
-
-
12
40
-
-
-
-
-
-
<5
440
-
-
-
<100
<100
<100
-
-
-
-
-
-
957
>147
-
7
1,000
-
<7
65
-
369
971
209
-
-
<5
11
-
-
-
-
-
-
<5
249
-
-
-
<100
<100
<100
-
-
-
-
-
-
958
>147
-
20
708
-
<7
18
-
129
2,410
785
-
-
<5
13
-
-
-
-
-
-
11
678
-
-
-
200
<100
<100
-
-
-
-
-
-
959
>147
_
9
22
-
<7
9
-
275
6.780
267
-
-
8
35
-
-
-
-
-
-
7
233
-
-
-
<100
<100
<100
-
-
-
-
-
-
960
>147
_
15
27
-
<7
119
-
300
1.550
537
-
-
<5
10
-
-
-
-
-
-
<5
446
-
-
-
<100
<100
<100
-
-
-
-
-
-
961
>147
_
11
36
-
<7
35
-
359
18,600
129
-
-
13
48
-
-
-
-
-
-
18
162
-
-
-
<100
<100
<100
-
-
-
-
-
-
962
>147
_
6
26
-
147
_
7
48
-
<7
153
-
442
2.660
122
-
-
<5
21
-
-
-
-
-
-
<5
102
-
-
<100
<100
<100
-
-
-
-
-
-
PNAs
Naphtnaiene
Penanthrene/Anthracene
Pyrene
Benzo(a)anthracene
Benzo(a)pyrene
Alkylbenzene (C.H )
Alkylnaphthalene tc12H12>
Phosphorus
Chlorine, wt %
Sulfur, wt Z
PCBs
0.04
-
5
0.04
-
6
0.16
<5
0.02
-
6
0.03
-
2
<0.01
-
2
0.03
-
3
0.01
-
4
* Table A-2 identifies the source of analytical data for each used oil sample. Table A-3 provides codes
for each sample number which describes the specific generating source of used oil and the end-use.
A-117
0292
-------
TABLE A-l (continued)
ANALYTICAL DATA FOR USED OIL SAMPLES
Flash Point (°F)
Metals
Aluminum
Arsenic
Barium
Beryllium
Cadmium
Chromium
Cobalt
Copper
Iron
Lead
Magnesium
Manganese
Molybdenum
Nickel
Selenium
Silicon
Silver
Sodium
Tin
Titanium
Vanadium
Zinc
Volatile Organics
Dichlorodifluoromethane
Trichlorofluoromethane
Trichlorotrifluoroethane
1,1,1-Trichloroethane
Trichloroethylene
Tetrachloroethylene
Phenol
Benzene
Toluene
Ethyl Benzene
Xylenes
Methylene Chloride
PNAs
Naphthalene
Penanthrene/Anthracene
Pyrene
Benzo(a)anthracene
Benzo(a)pyrene
Alkylbenzene (CgH..)
Alkylnaphthalene tc.-H.,)
Phosphorus
Chlorine, vt Z
Sulfur, ut Z
PCBs
964
84
<5
23
94
125
276
69
<5
<5
965
115
<5
178
39
2.730
720
15
7
966
>147
<5
105
<5
1,050
322
18
5
Sample Number*
967
>147
<5
32
8
26
189
273
<5
<5
968
93
14
107
16
51
796
476
8
<5
969
>147
<5
285
25
32
2,800
607
8
12
970
111
8
520
<10
27
37
21.100
563
25
72
971
97
<5
8
<5
38
43
<5
<5
<5
117
161
1.070
4,400 <100
<100 <100
300 <100
20
421
<100
<100
<100
7
495
2.500
<100
700
21
991
6.100
«100
<100
224
797
238
659
300 30.000
26.000 <100
200 200
<5
21
<100
<100
1.600
0.15
<50
0.22
0.19
0.29
1.31
<50
2.69
<20
2.94
<100
0.09
* Table A-2 identifies the source of analytical data for each used oil sample. Table A-3 provides codes
for each sample number which describes the specific generating source of used oil and the end-use.
A-118
-------
TABLE A-l (continued)
ANALYTICAL DATA FOR USED OIL SAMPLES
Sample Number*
Flash Point (°F)
Metals
Aluminum
Arsenic
Barium
Beryllium
Cadmium
Chromium
Cobalt
Copper
Iron
Lead
Magnesium
Manganese
Molybdenum
Nickel
Selenium
Silicon
Silver
Sodium
Tin
Titanium
Vanadium
Zinc
Volatile Organics
Dichlorodifluorome thane
Trichlorofluorome thane
Trichloro tr if luoroe thane
1,1, 1-Tr ichloroethane
Trichloroethylene
Tetrachloroethylene
Phenol
Benzene
Toluene
Ethyl Benzene
Xylenes
Methylene Chloride
972
>147
-
12
235
-
<10
18
-
<5
5,330
342
-
-
5
12
-
-
-
-
-
-
287
431
-
-
-
500
<100
200
-
-
-
-
-
-
9,73
>147
-
<5
106
-
<10
8
-
9
2,860
286
-
-
29
<5
-
-
-
-
-
-
78
795
-
-
-
400
<100
1,000
-
-
-
-
_
-
974
>147
-
23
70
-
<10
11
-
37
283
<5
-
-
<5
<5
-
-'
-
-
-
-
<5
773
-
-
-
500
<100
300
-
-
-
-
-
-
975
>126
-
<5
10
-
<10
<5
-
44
25
<5
-
-
<5
<5
-
-
-
-
-
-
<5
33
-
-
-
200
<100
<100
-
-
-
-
-
-
976
>147
-
<5
30
-
<10
<5
-
7
1,100
8
-
8
9
-
-
-
-
-
-
<5
14
-
-
-
1,600
<100
300
-
-
-
-
-
-
977
>147
-
<5
20
-
<10
22
-
199
717
9
-
-
9
<5
-
-
-
-
-
<5
165
-
-
-
700
<100
900
-
-
-
-
-
-
978
>147
-
<$,
10
-
<10
8
-
7
1,060
17
-
IV
<5
-
-
-
-
-
-
<5
36
-
-
-
<100
<100
1,400
-
-
-
-
-
-
979
>147
<5
10
-
<10
<5
9
550
<5
-
<5
<5
-
-
-
-
-
-
<5
<5
-
-
-
-
-
-
-
-
-
-
-
-
PNAs
Naphthalene
Penanthrene/Anthracene
Pyrene
Benzo(a)anthracene
Benzo(a)pyrene
Airiylbenzene (CgK..,)
Alkylnaphthalene t£H)
Phosphorus
Chlorine , wt %
Sulfur, wt I
PCBs
1.58
-
<50
0.42
-
<20
0.14
-
6
0.73 0.96
-
<1 <20
1.10
-
<20
1.01
-
<20
0.18
-
* Table A-2 identifies the source of analytical data for each used oil sample. Table A-3 provides codes
for each sample number which describes the specific generating source of used oil and the end-use.
A-119
0293
-------
TABLE A-l (continued.)
ANALYTICAL DATA FOR USED OIL SAMPLES
Sample Number*
Flash Point (°F)
Metals
Aluminum
Arsenic
Barium
Beryllium
Cadmium
Chromium
Cobalt
Copper
Iron
Lead
Magnesium
Manganese
Molybdenum
Nickel
Selenium
Silicon
Silver
Sodium
Tin
Titanium
Vanadium
Zinc
Volatile Organics
Dichlorodifluorome thane
Trichlorofluoromethane
T r ichl orotr if luoroe thane
1,1, 1-Trichloroethane
Trichloroethylene
Tetrachloroe thy lent
Phenol
Benzene
Toluene
E;h_. i Berizer.e
Xylenes
Methylene Chloride
980 981
>147 >147
- -
<5 <5
<10 20
-
<;o 147
_
<5
<10
-
<10
<5
-
<5
<5
6
-
-
<5
U7
-
8
30
-
<10
18
-
28
834
327
-
-
13
8
-
-
-
-
-
-
<5
267
-
-
-
800
<100
800
-
-
-
-
.
-
984
>U7
_
9
20
-
<10
<5
-
41
202
518
-
-
<5
147 >147
_
<5 <5
30 <10
>
<10 <10
<5 <5
_ _
6 <5
29 12
<5 12
-
-
<5 <5
<5 <5
-
-
_
_
-
_
<5 <5
17 330
-
.
-
1,200
<100
<100
- -
-
-
-
-
-
987
>147
_
21
<10
^
<10
8
_
12
222
747
-
-
<5
<5
_
-
_
_
_
_
<5
166
-
_
-
<100
<100
<100
_
-
-
-
-
-
PSAs
Naphthalene
Penanthrene/ Anthracene
Pyrer.e
Benzo(a)anthracene
Benzo(a)pyrene
Alkylbenzene (CgH..)
Alkvlnaohthalene TCH,,)
Phosphorus
Chlorine
Sulfur,
PCBs
, wt Z
wt 7.
0.04 <0.01 0.07
_
<1 - 44
0.73 0.66
-
<20 <10
0.09 0.16 0.05
_
<1 39
* Table A-2 identifies the source of analytical data for each used oil sample. Table A-3 provides codes
for each sample number which describes the specific generating source of used oil and the end-use.
A-l 20
-------
ANALYTICAL DATA FOR USED OIL SAMPLES
Sample Number*
Flash Point (°F)
Metals
Aluminum
Arsenic
Barium
Beryllium
Cadmium
Chromium
Cobalt
Copper
Iron
Lead
Magnesium
Manganese
Molybdenum
Nickel
Selenium
Silicon
Silver
Sodium
Tin
Titaniura
Vanadium
Zinc
Volatile Organics
D ..chlorodif luoromethane
Tricolor of luorome thane
Trichlorotrif luoroe thane
1, 1,1-Tnchloroethane
Trichloroethylene
Tecracr.loroethylene
Phenol
Benzene
Toluene
Ethyl Benzene
988
>147
-
<5
<10
-
<10
<5
-
<5
326
6
-
-
<5
<5
-
-
-
-
-
-
6
15
-
-
-
<100
<100
<100
-
-
-
-
989 990
>147 >147
- -
13 <5
80 30
-
<10 <10
431 168
- -
54 34
3,430 557
827 9
-
- -
<5 <5
8 6
-
-
-
-
-
- -
<5 8
263 273
-
-
-
1,000
5,400
6,100
-
-
-
-
991
>147
-
<5
10
-
<10
26
-
71
467
59
-
-
<5
<5
-
-
-
-
-
-
<5
23
-
-
-
400
<100
200
-
-
-
-
992
>147
-
<5
10
-
<10
10
-
229
415
58
-
-
<5
<5
-
-
-
-
-
-
<5
186
-
-
-
300
<100
400
-
-
-
-
993
>147
-
<5
50
-
<10
13
-
19
958
136
-
-
<5
<5
-
-
-
-
-
-
<5
211
-
-
-
1,100
<100
300
-
-
-
-
994
>147
-
<5
360
-
<10
104
_
218
6.020
259
-
-
12
24
-
-
-
-
-
-
36
650
-
-
-
300
<100
500
-
-
-
-
995
>147
-
<5
30
-
*10
42
_
220
1.900
86
-
<5
<5
-
-
-
-
-
-
<5
126
-
-
300
<100
400
-
-
-
-
Methyier.e Chloride
PN'As
Naphthalene
Penanthrene/Anthracene
Pvrene
3enzo(a;antnrace.r.e
Benzo(a)pyrene
Alkylbenzene (CgH,-)
Alkylnaphthalene tc.,H12)
Phosphorus
Chlorine, wt 7.
Sulfur, wt 2
PCBs
0.03
-
<5
0.62
-
53
0.14 0.39
- -
<50
0.78
<50
1.48
-
<50
1.66
-
<50
4.94
-
<50
* Table A-2 identifies the source of analytical data for each used oil sample. Table A-3 provides codes
aacn sample number which describes the specific generating source of used oil and the end-use.
A-121
0294
-------
TABLE A-l (concinuea;
ANALYTICAL DATA FOR USED OIL SAMPLES
Sample Number*
Flash Point (°F)
Metals
Aluminum
Arsenic
Barium
Beryllium
Cadmium
Chromium
Cobalt
Copper
Iron
Lead
Magnesium
Manganese
Molybdenum
Nickel
Selenium
Silicon
Silver
Sodvun
Tin
Titanium
Vanadium
Zinc
Volatile Organics
D ichlorod if luorome thane
Trichlorofluorome thane
Trichlorotrif luoroe thane
1 , 1 , 1-Trichloroethane
Trichloroethylene
Tetrachloroethylene
Phenol
Benzene
Toluene
Ethyl Senzer.e
Xylenes
Methylene Chloride
996
>147
.
33
30
-
<10
12
-
52
240
1,010
-
-
<5
<5
-
-
-
.
-
-
<5
1,030
-
-
-
100
<100
<100
_
-
-
-
-
-
997 996
99 >147
_
6 <5
<10 <9
-
<10 <5
8 <5
- -
20 13
229 <5
148 23
- -
-
<5 <6
15 <5
-
.
_
_ _
-
-
82 <5
37 391
-
-
-
<100 <100
<100 <100
<100 <100
- -
-
-
-
-
-
999
>U7
_
<5
81
-
<5
<5
_
6
23
81
-
<6
<5
-
_
-
_
_
_
<5
511
-
-
.
<100
<100
<100
.
.
-
-
-
-
1000
>147
«.
19
38
-
<5
12
_
47
137
625
-
-
<6
<5
-
.
-
_
.
-
<5
762
-
-
-
100
<100
<100
_
-
-
-
-
-
1001
>147
_
10
42
_
<5
<5
~.
106
139
273
-
_
<6
<5
_
_
_
_
..
_
<5
264
-
_
_
900
200
2,000
_
_
_
-
-
-
1002
120
_
<5
17
_
<5
<5
_
8
19
14
_
_
<6
<5
_
_
_
.
_
»
<5
30
-
.
_
8,200
<100
3.000
^
_
_
-
-
-
1003
>147
25
1.150
_
6
500
w
465
404
2.960
_
.
86
<5
_
v
-
.
559
268
_
_
_
1,700
<100
2.200
_
_
_
_
-
-
PSAs
Naphthalene
Penanthrene/Anthracene
Pyrene
Benzo(a)anthracene
Benzo(a)pyrene
Alkylbenzene (CgH,,)
Alkylnaphthalene tC.-H.,)
Phosphorus
Chlorine, wt Z
Sulfur, ut %
PCBs
0.12
0.07
0.01
0.08
0.07
<5
0.61
<50
0.77
<5
0.24
6
* Table A-2 identifies the sourc'e of analytical data for each used oil sample. Table A-3 provides codes
for each sample number which describes the specific generating source of used oil and the end-use.
A-122
-------
TABLE A-l (continued)
ANALYTICAL DATA FOR USED OIL SAMPLES
Sample Number*
Flash Point (CF)
Metals
Aluminum
Arsenic
Barium
Beryllium
Cadmium
Chromium
Cobalt
Copper
Iron
Lead
Magnesium
Manganese
Mrlybdenun
1004
72
<5
312
12
23
92
44
11
<5
1005
131
<5
240
7
104
56
18
<5
<5
109
19
39
161
94
<5
<5
1007
>147
<5
65
65
198
302
78
<5
<5
1008
XL47
<5
93
55
219
1,250
423
12
20
11
23
83
456
7
46
21
95
238
<5
<5
20
46
8
39
139
836
8
<5
Selenium
Silicon
Silver
Tin
Titanium
Vanadium
Zinc
<5
693
<5
1,150
<5
189
<5
78
8
221
<5
490
<5
206
<5
667
Volatile Organics
Dichlcrocifluoromethane
Trichlorofluoromethane
Trichlorocnfluoroe thane
1,1, i-Irichloroethane
Trichloroethylene
Tetrachloroethylene
Phenol
Benzene
Ztnyi Benzene
Xylenes
Methylene Chloride
PNAs
Naphthalene
Penanthrene/Anthracene
Pyrene
Benzo(a)anthracene
Ber.zo(a)pyrene
3,800 500
2.200 2,800
500 1,400
<100
<100
<100
<100
<100
<100
<100
<100
<100
<100
<100
<100
400 200
300 200
3,200 100
Alkylnapnthalene tc.-H^-)
Phosphorus
Chlorine, wt %
Sulfur, wt %
PCBs
0.42
0.32
0.40
16
0.47
38
0.19
83
0.45
64
2.25 0.16
* Table A-2 identifies the source of analytical data for each used oil sample. Table A-3 provides codes
:or each sample number which describes the specific generating source of used oil and the end-use.
A-l 23
0295
-------
TABLE A-l (continued)
ANALYTICAL DATA FOR USED OIL SAMPLES
Sample Number*
Flash Point (=F)
1012
>147
1013
>147
X014
>147
1015
>147
1016
>147
1017
>147
1018
>147
1019
>.147
Metals
Aluminum
Arsenic
Barium
Beryllium
Cadmium
Chromium
Cobalt
Copper
Iron
Lead
Magnesium
Manganese
Molybdenum
Nickel
Selenium
Silicon
Silver
Sodium
Tin
Titanium
Vanadium
Zinc
Volatile Organics
Dichlorodifluoromethane
Trichlorofluoromethane
Trichlorotrifluoroethane
1,1,1-Trichloroethane
Trichloroethylene
Tetrachloroethylene
Phenol
Benzene
Toluene
Etnyl Benzene
Xylenes
Methylene Chloride
PNAs
Naphthalene
Penanthrene/Anthracene
Pyrene
Benzo(a)anthracene
Benzo(a)pyrene
58
68
10
521
<5
14
<5
41
26
12
35
<5
8
<5
21
<5
6
27
<5
8
<5
<5
764
<5
21
<100 <100
1,500 12,000
<100 <100
<5
93
<100
<100
<100
Alkylbenzene (C.H
Alkylnaphthaler.e
Phosphorus
Chlorine, vt Z
Sulfur, wt 7.
PCBs
I2r'12'
< 5
399
50
95
2,150
3,250
14
23
27
51
44
158
856
<5
<5
24
25
<5
25
115
671
<5
<5
18
30
22
118
592
<5
<5
26
41
10
32
148
942
<5
<5
23 <5
2,030 730
1,600 <100
40,000 <100
<100 <100
<5
546
<100
<100
<100
<5
558
<5
830
<100 <100
<100 <100
<100 1.200
0.55
0.96
0.46
2.29
0.10
0.10
<5
0.21
0.14
* Table A-2 identifies the source of analytical data for each used oil sample. Table A-3 provides codes
for each sample number which describes the specific generating source of used oil and the end-use.
A-124
-------
TABLE A-l (continued;
ANALYTICAL DATA FOR USED OIL SAMPLES
Sample Number*
Flash Point CD
1020
>147
1021
>147
1022
>147
1023
>147
1024
>147
1025
>147
1026
>126
1027
>147
Metals
Aluminum
Arsenic
Barium
Beryllium
Cadmium
Chromium
Cobalt
Copper
Iron
Lead
Magnesium
Manganese
Molybdenum
Nickel
Selenium
Silicon
Silver
Sodium
Tin
Titanium
Vanadium
Zinc
Volatile Organics
Dichlorodifluoromechane
Trichlorofluoromethane
Trichlorotrifluoroethane
1,1,1-Tr ichloroe thane
Trichloroechylene
Tetrachloroethylene
Phenol
Benzene
Toluene
Etnyl Benzene
Xylenes
Methylene Chloride
PNAs
Naphthalene
Penanchrene/Anthracene
Pyrene
Benzo(a)anthracene
Benzo(a)pyrene
16
26
10
77
443
27
36
30
155
803
<5
<5
19
32
10
150
572
<5
<5
23
39
31
156
725
<5
<5
<5
428
<5
804
<100 <100
<100 <100
1,700 <100
<5
500
400
200
200
<5
622
Alkylbenzene (C,H
Alkylnaphthalene
Phosphorus
Chlorine, wt Z
Sulfur, wt %
PCBs
"12
0.13
0.10
0.27
0.36
<5
24
68
8
61
160
1,050
<5
<5
<5
788
2,200 1,100
600 1,200
<100 4.600
19
50
8
32
159
647
<5
<5
8
42
B
32
148
693
<5
<5
19
38
13
21
270
750
<5
<5
<5
694
<5
628
<5
683
400 2,600 <100
<100 1,800 <100
200 19,000 5.800
0.12
<5
2.96
<5
0.79
* Table A-2 identifies the source of analytical data for each used oil sample. Table A-3 provides codes
for each sample number which describes the specific generating source of used oil and the end-use.
A-125
029G
-------
TABLE A-i
ANALYTICAL DATA FOR USED OIL SAMPLES
Sample Number*
Flash Point (°F)
Metals
Aluminum
Arsenic
Barium
Beryllium
Cadmiun
Chromium
Cobalt
Copper
Iron
Lead
Magnesium
Manganese
Molybdenum
Nickel
Seleniur.
Silicon
Silver
Sodium
Tin
Titanium
Vanadium
Zinc
Volatile Organics
Dichlorodifluorooechane
Trichlorofluoromethane
Tnchlorotrif luoroethane
1 . 1 , 1-Trichloroethane
Tnchloroethylene
Tetrachloroethylene
Phenol
Benzene
Toluene
E:h-.-; Benzene
Xyleaes
Methylene Chloride
1028
>147
-
19
34
-
<10
<5
-
49
202
785
-
-
<5
<5
-
-
-
-
.
-
<5
864
-
-
-
8,400
<100
1,200
-
-
-
-
-
-
1029
>147
.
,28
39
-
<10
6
-
35
175
1,040
-
-
6
<5
-
-
-
-
-
-
<5
1.020
-
-
-
500
<100
200
-
-
-
-
-
1030
>147
-
19
28
-
<10
<5
-
11
194
555
-
-
<5
<5
-
-
-
-
_
-
<5
321
-
-
-
3,400
300
5,800
-
-
-
_
-
-
1031
>147
-
94
160
-
<10
<5
_
11
1.410
2.480
-
-
7
11
-
.
_
-
_
_
12
2,670
-
-
-
1,100
200
1,500
_
-
-
-
-
-
1032
>147
_
9
243
_
<10
66
_
40
992
786
-
-
14
17
_
-
-
-
_
_
7
1,480
-
_
.
800
500
1,100
-
-
-
_
-
-
1033
>147
_
26
38
_
<10
<5
37
160
1,010
-
_
6
<5
_
_
.
_
_
_
<5
848
_
_
-
700
300
300
_
_
.
_
-
-
1034
>147
_
32
32
<10
<5
_
36
151
932
_
_
5
<5
»
_
_
_
_
_
<5
625
_
_
_
2.600
400
2.200
_
_
_
_
-
-
1035
>147
17
45
. ,
<10
10
50
180
826
_
_
<5
<5
_
.
^,
w
<5
716
.
^
_
2,400
3,000
8,200
_
_
_
-
-
PNAs
Naphthalene
Penanthrene/Anthracene
Pyrene
Benzo(a)anthracene
Benzo(a)pyrene
Alkylbenzene (Cgfc
AlkyInaphthalene
Phosphorus
"12
Chlorine,
wt Z
0.29 0.10 1.06 0.09 0.22 0.20
0.25
1.85
Sulfur , ut % ________
PCBs
<5
<5
* Table A-2 identifies the source of analytical data for each used oil sample. Table A-3 provides codes
ror eacr. sample number which describes the specific generating source of used oil and the end-use.
A-126
-------
ANALYTICAL DATA FOR USED OIL SAMPLES
Sample Table*
Flash Point (T) .
Metals
Aluminum
Arsenic
Barium
Beryllium
Cadmium
Chromium
Cobalt
Copper
Iron
Lead
Magnesium
Manganese
Molybaer.'-r:
Nicicel
Selenium
Silicon
Silver
Sodium
Tin
Titanium
Vanadium
Zinc
Volatile Organics
Dichlorod if luorome thane
Trichlorofluorome thane
Tr ichlorotr if luoroe thane
1,1,1-Inchloroethane
Tnchloroethvlene
Tetracnioroethylene
Phenol
Benzene
Toluene
Ethyl Benzene
Xvlenes
Meth;. lene Chloride
1036
>147
-
22
37
-
<10
6
57
167
864
-
-
<5
<5
-
-
-
-
-
-
<5
709
-
-
-
4,200
200
1,100
-
-
-
-
-
-
1037
>147
-
<5
85
-
<10
25
_
27
615
177
-
-
<5
8
-
-
-
-
-
-
10
273
-
-
-
1,300
<100
32.000
-
-
-
-
-
1036 1039
135
-
<5 17
19 40
-
<10 <10
<5 27
-
7 24
48 146
5 558
-
-
<5 <5
<5 <5
-
-
-
-
-
-
<5 <5
15 527
-
-
-
4,200
1,900
2,000
- -
-
-
-
-
-
1040
136
_
29
50
-
<10
18
_
39
297
885
-
-
7
<5
-
-
-
-
-
-
10
728
-
-
5,200
1,600
2,400
-
-
-
-
-
-
1041
>147
_
24
30
-
<10
16
_
41
146
771
.
-
<5
<5
-
-
-
-
-
-
<5
575
-
-
.
6,000
900
2,800
-
-
-
~
-
-
1042
>147
_
~i "i
40
-
<10
12
_
41
143
901
-
_
<5
<5
-
-
-
-
-
_
<5
631
_
-
_
14,000
600
2,600
-
-
-
-
-
1043
108
_
11
40
-
<10
16
_
44
155
603
.
-
<5
<5
-
-
-
-
-
-
<5
1 525
t
_
_
_
14,000
3,000
6,800
-
-' -
-
-
_
-
PN'As
Naphthalene
Penantnrene/Anthracene
Pyrene
Benzo(a)anthracene
Benzo(a)pyrene
Alkylbenzene (CgH.,)
Alkylnaphthalene TC.,H..)
Phosphorus
Chlorine, wt %
Sulfur, wt X
PCBs
0.56
<5
2.74
0.46
0.95
1.04
1.00
1.44
l.lk
* Table A-2 identifies the source of analytical data for each used oil sample. Table A-3 provides codes
for each sample number which describes the specific generating source of used oil and the end-use.
A-127
0297
-------
TABLE A-l (continued)
ANALYTICAL DATA FOR USED OIL SAMPLES
Sample N\aiber*
Flash Point (*F)
Metals
Aluminum
Arsenic
Barium
Beryllium
Cadmium
Chromium
Cobalt
Copper
Iron
Lead
Magnesium
Manganese
Molybdenum
Nickel
Selenium
Silicon
Silver
Sodium
Tin
Titanium
Vanadium
Zinc
Volatile Organics
Dichlorodifluoromethane
trichlorof luor omethane
Trichlorotrif luoroethane
1 > 1 , 1-Tr ichloroe thane
Trichloroethylene
Tetrachloroethylene
Phenol
Benzene
Toluene
Ethyl Benzene
Xylenes
Methylene Chloride
1044
135
-
22
40
-
<10
16
44
159
637
-
-
<5
<5
-
-
-
-
-
-
<5
664
-
-
-
3,300
900
r.soo
-
.
-
-
-
-
1045
66
-
<5
<5
-
<10
<5
.
<5
11
17
-
-
<5
<5
-
-
-
-
-
-
<5
5
-
-
-
3,400
<100
600
-
-
-
-
-
-
j.046
64
_
<5
20
-
<10
<5
_
<5
11
21
-
-
<5
<5
-
-
-
-
-
-
<5
6
-
-
.
2,000
<100
400
-
-
-
-
-
-
1047
115
.
<5
<5
-
<10
<5
_
<5
10
24
-
-
<5
<5
-
-
-.
-
-
-
<5
65
-
-
-
1,800
700
1.200
-
-
-
-
-
-
1048
120
_
21
40
-
<10
28
»
40
170
688
-
-
<5
<5
-
-
_
-
-
-
<5
530
_
-
-
6,600
700
1,300
-
-
-
-
-
-
1049
>147
_
<5
170
_
10
35
_
126
1,250
1.820
-
-
10
7
«
-
_
_
_
29
1,770
_
-
-
200
<100
200
.
_
-
-
-
-
1050
>147
18
180
_
<10
56
138
367
531
.
_
<5
<5
_
_
.
_
_
_
34
591
_
-
_
2,600
200
700
.
_
.
-
-
-
1051
113
20
50
_
<10
18
^
35
185
656
_
_
<5
<5
_
.
_
_
_
*
15
478
_
-
_
4,600
500
700
.
_
_
-
-
-
PSAs
Naphthalene
Penanthrene/ Anthracene
Pyrene
Benzo (a) anthracene
Benzo(a)pyrene
Alkylbenzene (C.H.
Alkylnaphthalene t
)
Phosphorus
Chlorine, wt Z
Sulfur, wt 2
PCBs
--._.._
0.77 0.16 0.10 0.17 0.87 0.15
_______
<10 4 2 <1 <10 <10 <10
-
0.91
-
* Table A-2 identifies the source of analytical data for each used oil sample. Table A-3 provides codes
for each sample number which describes the specific generating source of used oil and the end-use.
A-l 28
-------
ANALYTICAL DATA FOR USED OIL SAMPLES
Sample Number*!
Flash Point (°F)
Metals
Aluminum
Arsenic
Barium
Beryllium
Cadmiuc
Chromium
Cobalt
Copper
Iron
Lead
Magnesium
Manganese
Molybdenum
Nickel
Seleniur.
Silicon
Silver
Sodium
Tin
Titaniun
Vanadiuc
Zinc
Volatile Organics
Dichlorodifluoromethane
Trichlcrof luoromethane
Trichlorocrif luoroe thane
1 ,1,1-Trichloroethane
Trichloroetnylene
Tetracnloroethylene
Phenol
Benzene
Toluene
Ethvl Benzene
Xy.er.ss
Methylene Chloride
1052
>147
-
12
20
-
<10
<5
-
<7
7
<5
-
-
10
<5
-
-
-
-
-
<5
8
-
-
-
<100
<100
<100
-
-
-
-
-
-
1053
>147
-
13
190
-
10
35
-
91
1,440
2.180
-
-
7
7
-
-
-
-
-
38
1,870
-
-
-
2,800
200
800
-
-
-
-
-
-
1054
>147
-
16
90
-
<10
84
-
174
126
6-: 6
-
*
<5
<5
-
-
-
-
*
-
<5
269
-
-
-
6,200
800
1,400
-
-
-
-
-
-
1055
135
-
22
40
-
<10
29
-
146
205
768
-
- .
<5
<5
-
-
-
-
-
5
514
-
-
-
3,000
600
600
-
-
-
-
-
-
1056(80) 1057(81)
>200
45
<5
67
<0.2
1.1
6.1
<0.5
33
300
890
150
10
3.3
_
110
5
310
-
-
-
1.800
460
400
-
150
2,000
430
820
250
<85
7.6
<5
25
<0.2
0.66
1.9
<0.5
25
130
440
23
3
1.4
_
_
11
_
3.7
370
-
-
-
450
120
800
-
12,000
8,000
4,000
25,000
1,400
1058(82)
>200
16
<5
35
<0.2
2.9
2.2
<0.5
26
99
560
74
4.6
1.1
9.1
1.5
730
-
-
-
1,500
390
380
-
160
670
200
500
12
1059(83
>200
23
<5
47
3.7
2. 8
<0.5
27
110
770
110
5.7
1.2
21
0.79
860
-
-
-
1,000
<4
15
-
240
810
270
50C
7
PNAs
Naphthalene
Penan threne/ Anthracene
Pyrene
Benzo (a) anthracene
Benzo(a)pyrene
AlKylbenzene (Cg
Alkylnaphthalene
Phosphorus
Chlorine, wt %
Sulfur, wt Z
PCBs
' 640
0.12 0.29 0.68 0.51 0.07
0.63
440
0.21
<°5'37
660
0.33
710
0.1
* Table A-2 identifies the source of analytical data for each used oil sample. Table A-3 provides codes
for each sample number which describes the specific generating source of used oil and the end-use.
t Numbers in parentheses represent EPA sample numbers for used oil samples obtained as part of their
1983 sampling program.
A-129
0298
-------
ANALYTICAL DATA FOR USED OIL SAMPLES
Flash Point (°F)
Metals
Aluminum
Arsenic
Barium
Beryllium
Cadmium
Chromium
Cobalt
Copper
Iron
Lead
Magnesium
Manganese
Molybdenum
N'ickel
Selenium
Silicon
Silver
Sodium
Tin
Titanium
Vanadium
Zinc
Volatile Organics
Dichlorodifluoromethane
Trichlorofluoromethane
Trichlorotrifluoroethane
1,1,1-Trichloroethane
Trichloroethylene
Tetrachloroethylene
Phenol
Benzene
Toluene
Xylenes
Methylene Chloride
PSAs
Naphthalene
Phenanthrene/Anthracene
Pyrer.e
Benzo(a)anthracene
Benzo(a)pyrene
Alkylbenzene (C
Alkylnaphthalene
Sample Number* t
1060 (84) 1061 (85) 1062 (86) 1063 (358) 1064 (361) 1065 (306)
>200 >200 >200 >200 104
3.6
<5
13
<0.2
0.93
1.6
<0.5
16
97
610
76
2.6
16
<5
52
<0.2
4.1
2.9
<0.5
27
100
720
170
5.9
11
<5
<0.5
<0.2
1.7
2.1
<0.5
7.6
75
<5
3.7
0.59
<1
<5
<0.5
<0.2
0.83
9.5
0.73
<0.5
130
<5
1.5
<0.2
2.1
48
4.2
520
<1
35
0.36
820
11
<0.2
3.7
3.2
<0.2
2.4
3,500
<4
4
97
640
200
7
<4 .
44
<2
3
3
86
88
111
<2
140
<1
-------
ANALYTICAL DATA FOR USED OIL SAMPLES
Sample Number* t
Flash Point (*F)
Metals
Aluminum
Arsenic
Barium
Beryllium
Cadmium
Chromium
Cobalt
Copper
Iron
Lead
Magnesium
Manganese
Mciyocenua
Nickel
Selenium
Silicon
Silver
Sodium
Tin
Titanium
Vanadium
Zinc
Volatile Organics
Dichlorodif luoromethane
Trichlorof luoromethane
Trichlorotrifluoroe thane
1,1, 1-Trichloroe thane
Trichloroethylene
Tetrachloroethylene
Phenol
Benzene
Toluene
Ethyl Benzene
Xyler.cs
Methylene Chloride
1066 (34)
-
980
<5
3.2
<0.2
<0.5
1.5
<0.5
<0.5
5.1
<5
0.69
0.34
-
<1
-
-
-
2.1
-
-
0.2
2.6
-
-
-
<20
<20 26
<20
-
<20
230
<20
<20
<20 26
1067 (36) 1068 (37) 1069 (50) 1070:54)
-
<1
<5
3.2
<0.2
<0.5
6.7
3.5
18
74
100
0.99
49
-
8.1
-
-
-
11
-
-
<0.2
38
-
.
-
<20
,000
<20
-
<20
<20
670
560
,000
-
8.7
<5
120
<0.2
<0.5
2.8
<0.5
3.4
87
<5
15
3.5
-
<1
-
-
-
2.4
-
_
0.49
10
-
-
-
<8
<8
<8
-
<8
<8
<8
<8
<8
>200
53
<5
8.5
<0.2
<0.5
7
<0.5
5.4
350
13
17
2
-
<1
_
-
.
1,800
-
_
<0.2
3.9
-
_
-
<7.4
<7.4
<7.4
-
<7.4
<7.4
<7.4
<7.4
<7.4
-
<1
<5
1.1
<0.2
<0.5
<0.5
<0.5
14
8.2
16
<0.5
0.49
-
1.5
_
_
-
1.3
-
_
<0.2
23
-
_
-
<16
<16
<16
-
<16
<16
<16
<16
<16
1071(59)
>200
16
<5
8.5
<0.2
<0.5 -"
0.82
0.93
19
110
6.9
0.56
0.62
-
1.1
_
_
-
2.4
-
_
<0.2
14
-
_
_
<32
<32
<32
-
<32
57
<32
<32
<32
PNAs
Naphthalene
Penanthrene/Anthracene
Pyrene
Benzo(a)anthracene
Benzo(a)pyrene
Alkylbenzene (CqH..,)
Alkylnaphthalene tc,,H,,)
Phosphorus
Chlorine, wt 2
Sulfur, wt Z
PCBs
300
<0.01
<5
580
0.93
<5
280
2
<5
380
0.02
0.51
<5
110
0.01
<5
270
0.65
<5
* Table A-2 identifies the source of analytical data for each used oil sample. Table A-3 provides codes
for each sample number which describes the specific generating source of used oil and the end-use.
+ Numbers in parentheses represent EPA sample numbers for used oil samples obtained as part of their
1983 sampling program.
A-132
0293
-------
TABLE A-2
SOURCE KEY FOR USED OIL SAMPLES IN TABLE A-l
Sample
Number
1-7
8
9
10
11-20
21
22-43
except 26
26
44
45
46
47
48
49
50
51
52-63
Source
A-l
A-12
A-12
A-10
A-2
A-13
A-15
A-21
A-17
A-26
A-27
A-28
A-29
A-30
A- 34
A-32
A-38
Date of
Publication
or Analysis
1982
1976
1981
Unknown
1977
1972
1977
1982
1979
1977
1977
1974
1974
1976
1981
1980
1978
A-133
-------
TABLE A-2 (continued)
SOURCE KEY FOR USED OIL SAMPLES IN TABLE A-l
Sample
Number
64
65-66
67-69
70-72
73-92
93-94
95-112
113-134
135-137
138
139
140
141
142
143
144
145
146
147
Source
A-39
A-36
A-37
A-48
A-32
A-24
A-24
A-24
A-19
A-l 9
A-19
A-19
A-19
A-19
A-19
A-19
A-19
A-19
A-40
Date of
Publication
or Analysis
1982
1982
1974
1983
1980
1978
1978
1978
Unknown
Unknown
1978
1978
1978
1978
1978
1978
1978
1978
1982
A-134
0300
-------
TABLE A-2 (continued)
SOURCE KEY FOR USED OIL SAMPLES IN TABLE A-l
Sample
Number
148
149
150
151
152
153
154
155
156
157
158
159
160
161-162
163-176
177
178
179
180-236
Source
A-40
A-40
A-40
A-40
A-40
A-40
A-40
A-40
A-40
A-40
A-40
A-40
A-40
A-25
A-49
A-5
A-10
A-10
A-20
Date of
Publication
or Analysis
1982
1982
1982
1982
1982
1982
1982
1982
1982
1982
1982
1982
1982
1977
1983
1982
Unknown
Unknown
1979-1981
A-135
-------
TABLE A-2 (continued)
SOURCE KEY FOR USED OIL SAMPLES IN TABLE A-l
Sample
Number
237-243
244
245
246-253
254-258
259-260
261
262-263
264-266
267
268
269-315
316-317
318-334
335-404
405-431
432-459
460-481
Source
A-l
A-3
A-4
A-9
A-20
A-7
A-ll
A-9
A-5
A-22
A-22
A-23
A-35
A-8
A-20
A-42
A-4 3
A-44
Date of
Publication
or Analysis
1982
1977
1979
1981
1981
1981
1979
1981
1982
1982
1982
1982
1982
1982
1979 to 1981
1982
1982
1982
A-136
0301
-------
TABLE A-2 (continued)
SOURCE KEY FOR USED OIL SAMPLES IN TABLE A-l
Sample
Number
482-490
491-568
569-578
579-589
590
591
592-659
660-669
670-737
738-771
772-839
840-879
880-1055
Source
A-45
A-49
A-32
A-9
A-47
A-47
A-48
A-46
A-48
A-49
A-48
A-50
A-49
Date of
Publication
or Analysis
1982
1983
1980
1981
1982
1974
1983
1983
1983
1983
1983
1978
1983
A-137
-------
TABLE A-3
USED OIL SAMPLE IDENTIFICATION CODES
SAMPLE
NUMBER
1
2
3
4
5
6
7
8
9
10
11
12
13
14
15
16
17
18
19
20
21
22
23
24
25
26
27
28
29
30
31
32
33
34
35
36
37
38
39
40
CODE*
C, J
C, J
C, J
C, J
C, J
C, J
C, J
B, J
B, J
B, J
B, H
B, H
B, H
B, H
B, H
B, H
B, H
B, H
B, H
C, J
C, J
B, J
B, J
B, J
B, J
C, G
B, J
B, J
B, J
B, J
B, J
B, J
B, J
B, J
B, J
B, J
B, J
B, J
B, J
B, J
SAMPLE
NUMBER
41
42
43
44
45
46
47
48
49
50
51
52
53
54
55
56
57
58
59
60
61
62
63
64
65
66
67
68
69
70 (262) t
71 (263)
72 (264)
73
74
75
76
77
78
79
80
CODE
B, J
B, J
B, J
B, J
B, J
C, H
B, J
B, J
B, J
C, G
B, J
B, H
B, H
B, H
B, H
B, H
B, H
B, H
B, H
B, H
B, H
B, H
B, H
C, G
C, J
C, J
C, J
C, J
C, J
A, C, J, K
A, C, J, K
A, C, J, K
B, G
B, G
B, G
B, G
B, G
B, G
B, G
B, G
* Letter codes are defined at end of table.
f Numbers in parentheses represent EPA sample numbers for used oil
samples obtained as part of their 1983 sampling program.
A-138
0302
-------
TABLE A-3 (continued)
USED OIL SAMPLE IDENTIFICATION CODES
SAMPLE
NUMBER
81
82
83
84
85
86
87
88
89
90
91
92
93
94
95
96
97'
98
99
100
101
102
103
104
105
106
107
108
109
110
111
112
113
114
115
116
117
118
119
120
CODE*
B, G
B, G
B, G
B, G
B, G
B, G
B, G
B, G
B, G
B, G
B, G
B, G
Dl, J
Dl, J
E4, il
E4, H
E4, H
E4, H
E4, H
E4, H
E4, H
E4, H
E4, H
E4, H
E4, H
E4, H
E4, H
E4, H
E4, H
E4, H
E4, H
E4, H
Dl, J
D4, J
Dl, J
Dl, J
D4, J
Dl, J
Dl, J
Dl, J
SAMPLE
NUMBER
121
122
123
124
125
126
127
128
129
130
131
132
133
134
135
136
137
138
139
140
141
142
143
144
145
146
147
148
149
150
151
152
153
154
155
156
157
158
159
160
CODE
Dl, J
Dl, J
Dl, J
Dl, J
Dl, J
Dl, J
Dl, J
Dl, J
Dl, J
Dl, J
Dl, J
D4, J
D4, J
DA, J
D4, J
D4, J
D4, J
Dl, J
Dl, J
D4, J
D4, J
D4, J
D4, J
D4, J
D4, J
D3, J
Dl, J
Dl, J
D3, J
Dl, J
Dl, J
Dl, J
D2, J
Dl, J
Dl, J
Dl, J
D4, J
Dl, J
Dl, J
Dl, J
* Letter codes are defined at end of table.
A-139
-------
TABLE A-3 (continued)
USED OIL SAMPLE IDENTIFICATION CODES
SAMPLE
NUMBER
161
162
163
164
165
166
167
168
169
170
171
172
173
174
175
176
177
178
179
180
181
182
183
184
185
186
187
188
189
190
191
192
193
194
195
196
197
198
199
200
CODE*
D4, J
D4, J
E4, G
E4, G
E4, G
E4, G
E4, G
E4, G
E4, G
E4, G
E4, G
E4, G
E4, G
E4, G
E4, G
E4, G
D4, J
D4, J
D4, J
F, I
F, I
F, I
F, I
F, I
F, I
F, I
F, I
F, I
F, I
F, I
F, I
F, I
F, I
F, I
F, I
F, I
F, I
F, I
F, I
F, I
SAMPLE
NUMBER
201
202
203
204
205
206
207
208
209
210
211
212
213
214
215
216
217
218
219
220
221
222
223
224
225
226
227
228
229
230
231
232
233
234
235
236
237
238
239
240
CODE
F, I
F, I
F, I
F, I
F, I
F, I
F, I
F, I
F, I
F, I
F, I
F, I
F, I
F, I
F, I
F, I
F, I
F, I
F, I
F, I
F, I
F, I
F, I
F, I
F, I
F, I
F, I
F, I
F, I
F, I
F, I
F, I
F, I
F, I
F, I
F, I
F, J
F, J
F, J
F, J
Letter codes are defined at end of table.
A-140
0303
-------
TABLE A-3 (contintied)
USED OH. SAMPLE IDENTIFICATION
SAMPLE
»uriBER
241
242
243
244
245
246
247
248
249
250
251
252
253
254
255
256
257
258
259
260
261
262
263
264
265
266
267
268
269
270
271
272
273
274
275
276
277
278
279
280
CODE*
F, J
F, J
-F. J
F, J
F, J
F, T>
F, D
F, D
F, D
F, D
T. D
F, JD
F, D
F, D
F, D
F, D
F, D
F, D
F, I
F, I
F, I
F, T
F, I
F, H
F, B
F, H
F, H
F, H
F, H
F. H
F. H
F. H
F, H
F, H
F, H
F, H
F, H
F, H
T, B
T, H
SAMPLE
UUMBER
281
282
283
284
285
286
287
288
289
290
291
292
293
294
295
296
297
298
299
300
301
302
303
304
305
306
307
308
309
310
311
312
313
314
315
316
317
318
319
320
CODES
CODE
F, G
F, G
F, G
F, G
F, G
F, G
F, G
F, G
F, G
F, G
F, G
F, G
F, G
F, G
F, G
F, G
F, G
F, G
F, G
F, G
F, G
F, G
F, G
F, G
F, G
F, G
F, G
F, G
F, G
F, G
F, G
F, G
F, G
F, G
F, G
F, G
F, G
F, P
F, P
F, P
Letter codes are defined at end of table.
A-141
-------
TABLE A-3 (continued)
USED OIL SAMPLE IDENTIFICATION CODES
SAMPLE
NUMBER
321
322
323
324
325
326
327
328
329
330
331
332
333
334
335
336
337
338
339
340
341
342
343
344
345
346
347
348
349
350
351
352
353
354
355
356
357
358
359
360
CODE*
F, P
F, P
F, P
F, P
F, P
F, P
F, P
F, P
F, P
F, P
F, P
F, P
F, P
F, D
F, I
F, I
F, I
F, I
F, I
F, I
F, I
F, I
F, I
F, I
F, I
F, I
F, I
F, I
F, I
F, I
F, I
F, I
F, I
F, I
F, I
F, I
F, I
F, I
F, I
F, I
SAMPLE
NUMBER
361
362
363
364
365
366
367
368
369
370
371
372
373
374
375
376
377
378
379
380
381
382
383
384
385
386
387
388
389
390
391
392
393
394
395
396
397
398
399
400
CODE
F, I
F, I
F, I
F, I
F, I
F, I
F, I
F, I
F, I
F, I
F, I
F, I
F, I
F, I
F, I
F, I
F, I
F, I
F, I
F, I
F, I
F, I
F, I
F, I
F, I
F, I
F, I
F, I
F, I
F, I
F, I
F, I
F, I
F, I
F, I
F, I
F, I
F, I
F, I
F, I
* Letter codes are defined at end of table.
A-142
0304
-------
TABLE A-3 (continued)
USED OIL SAMPLE IDENTIFICATION CODES
SAMPLE
NUMBER
401
402
403
404
405
406
407
408
409
410
411
412
413
414
415
416
417
418
419
420
421
422
423
424
425
426
427
428
429
430
431
432
433
434
435
436
437
438
439
440
CODE*
F, I
F, I
F, I
F, I
F, G
F, G
F, G
F, G
F, G
F, G
F, G
F, G
F, G
F, G
F, G
F, G
F, G
F, G
F, G
F, G
F, G
F, G
F, G
F, G
F, G
F, G
F, G
F, G
F, G
F, G
F, G
F, G
F, G
F, G
F, G
F, G
F, G
F, G
F, G
F, G
SAMPLE
NUMBER
441
442
443
444
445
446
447
448
449
450
451
452
453
454
455
456
457
458
459
460
461
462
463
464
465
466
467
468
469
470
471
472
473
474
475
476
477
478
479
480
CODE
F, G
F, G
F, G
F, G
F, G
F, G
F, G
F, G
F, G
F, G
F, G
F, G
F, G
F, G
F, G
F, P
F, P
F, G
F, G
F, G
F, G
F, G
F, G
F, G
F, G
F, G
F, G
F, G
F, G
F, G
F, G
F, G
F, G
F, G
F, G
F, G
F, G
F, G
F, G
F, G
* Letter codes are defined at end of table.
A-143
-------
TABLE A-3 (continued)
USED OIL SAMPLE IDENTIFICATION CODES
SAMPLE
NUMBER
481
482
483
484
485
486
487
488
489
490
491
492
493
494
495
496
497
498
499
500
501
502
503
504
505
506
507
508
509
510
511
512
513
514
515
516
517
518
519
520
CODE*
F,
F,
F,
F,
F,
F,
F,
F,
F,
F,
F,
F,
F,
F,
F,
F,
F,
F,
F,
F,
F,
F,
F,
F,
F,
F,
F,
F,
F,
F,
F,
F,
F,
F,
F,
F,
F,
F,
F,
F,
G
G
G
G
G
G
G
G
G
G
G,
G,
G,
G,
G,
G,
G,
G,
G,
G,
G,
G,
G,
G,
G,
G,
G,
G,
G,
G,
G,
G,
G
G
G,
G
G
G
G
G,
L
L
L
L
L
L
L
L
R
K
R
L
L
L
L
L
L
L
L
R
R
L
R
L
SAMPLE
NUMBER
521
522
523
524
525
526
527
528
529
530
531
532
533
534
535
536
537
538
539
540
541
542
543
544
545
546
547
548
549
550
551
552
553
554
555
556
557
558
559
560
CODE
F
F
F
F
F
F
F
F
F
F
F
F
F
F
F
F
F
F
F
F
F
F
F
F
F
F
F
F
F
F
F
F
F
F
F
F
F
F
F
F
9
9
9
9
9
9
9
9
9
9
9
9
9
9
9
9
9
9
9
9
9
9
9
9
9
9
9
9
9
9
9
9
9
9
9
9
9
9
9
9
G
G
G
G
G
G
G
G
G
G
G
G
G
G
G
G
G
G
G
G
G
G
G
G
G
G
G
G
G
G
G
G
G
G
G
G
G
G
G
G
9
9
9
9
9
9
f
9
9
9
9
9
9
9
9
9
9
9
»
9
9
9
9
9
9
9
9
9
9
9
9
9
9
9
9
9
9
9
9
9
L
L
L
L
L
L
R
R
R
L
L
L
L
L
R
R
R
R
R
R
R
R
R
R
L
L
L
L
L
R
R
R
R
R
R
R
R
K
R
R
* Letter codes are defined at end of table.
A-144
0305
-------
TABLE A-3 (continued)
USED OIL SAMPLE IDENTIFICATION CODES
SAMPLE
NUMBER
561
562
563
564
565
566
567
568
569
570
571
572
573
574
575
576
577
578
579
580
581
582
583
584
585
586
587
588
589
590
591
592 (H0)t
593 (111)
594 (112)
595 (118)
596 (119)
597 (120)
598 (121)
599 (123)
600 (124)
CODE*
F,
F,
F,
F,
F,
F,
F,
F,
F,
F,
F,
F,
F,
F,
F,
F,
F,
F,
F,
F,
F,
F,
F,
F,
F,
F,
F,
F,
F,
F,
F,
A,
A,
A,
A,
A,
A,
A,
A,
A,
G,
G,
G,
G,
G,
G,
G,
G,
H
H
H
H
H
H
H
H
H
H
J
J
J
J
J
J
J
J
J
J
J
I
J
B,
B,
B,
B,
D3
B,
B,
B,
B,
K
K
K
K
K
K
K
K
J, K
J, K.
J, K
J, K
, K, J
J, K
J, K
J > K
J, K
SAMPLE
NUMBER
601
602
603
604
605
606
607
608
609
610
611
612
613
614
615
616
617
618
619
620
621
622
623
624
625
626
627
628
629
630
631
632
633
634
635
636
637
638
639
640
(125)
(126)
(127)
(128)
(129)
(130)
(131)
(132)
(133)
(135)
(137)
(138)
(140)
(142)
(146)
(147)
(148)
(151)
(152)
(161) .
(163)
(164)
(165)
(166)
(167)
(168)
(169)
(170)
(174)
(177)
(181)
(182)
(187)
(188)
(190)
(191)
(193)
(202)
(204)
(205)
CODE
A,
A,
A,
A,
A,
A,
A,
A,
A,
A,
A,
A,
A,
A,
A,
A,
A,
A,
A,
A,
A,
A,
A,
A,
A,
A,
A,
A,
A,
A,
A,
A,
A,
A,
A,
A,
A,
A,
A,
A,
B
B
B
B
B
B
B
B
B
F
F
F
F
F
F
F
C
C
C
F
F
F
F
F
F
F
F
F
F
F
F
F
F
F
F
F
F
F
>
t
»
>
>
»
»
»
»
>
t
>
>
»
»
»
»
t
t
*
»
>
>
t
»
t
>
t
t
»
t
f
>
»
»
t
t
>
DA
D4
J
J
J
J
J
J
J
J
J
H
H
H
H
H
H
H
G
G
G
J
J
J
J
J
I
I
I
I
I
J
J
J
J
J
J
G
J
J
»
»
»
t
»
»
»
t
>
»
>
>
>
>
>
>
»
»
>
>
»
»
»
t
>
f
>
>
>
«
»
>
»
>
J
J
K
K
K
K
K
K
K
K
K
K
K
L
K
K
K
K
K
K
K
K
K
K
K
K
K
K
K
K
K
K
K
K
K
, K
, K
* Letter codes are defined at end of table.
t Numbers in parentheses represent EPA sample numbers for used oil
samples obtained as part of their 1983 sampling program.
A-145
-------
TABLE A-3 (continued)
USED OIL SAMPLE IDENTIFICATION CODES
SAMPLE
NUMBER
641 (207)t
642 (208)
643 (209)
644 (233)
645 (242)
646 (243)
647 (245)
648 (250)
649 (255)
650 (256)
651 (257)
652 (258)
653 (259)
654 (261)
655 (265)
656 (267)
657 (268)
658 (271)
659 (272)
660
661
662
663
664
665
666
667
668
669
670 (13)
671 (14)
672 (15)
673 (16)
674 (60)
675 (104)
676 (105)
677 (106)
678 (107)
679 (108)
680 (109)
CODE*
A, F, J, L
A, F, J, L
A, F, J, L
A, F, J, K
A, D3, J, K
A, D4, J, K
A, D4, J, K
A, E3, J, K
A, F, J, K
A, F, J, K
A, F, J, K
A, F, J, K
A, B, J, K
A, B, J, K
A, E4, J, K
A, E4, G, K
A, F, J
A, C, H, K
A, C, J, K
F, G
F, G
F, G
F, G
F, G
F, G
F, G
F, G
F, G
F, G
A, D4, J
A, D4, J
A, D4, J
A, D4, J
A, B, G
A, F, G
A, F, G
A, F, G
A, F, G
A, F, G
A, F, G
SAMPLE
NUMBER
681 (211)
682 (212)
683 (213)
684 (218)
685 (220)
686 (227)
687 (228)
688 (230)
689 (280)
690 (281)
691 (282)
692 (284)
693 (285)
694 (288)
695 (292)
696 (294)
697 (295)
698 (296)
699 (298)
700 (299)
701 (300)
702 (301)
703 (302)
704 (303)
705 (316)
706 (319)
707 (145)
708 (171)
709 (172)
710 (173)
711 (175)
712 (176)
713 (178)
714 (179)
715 (183)
716 (184)
717 (185)
718 (186)
719 (192)
720 (194)
i
CODE
A, J, J
A, J, J
A, F, J
A, D3, J
A, D3, J
A, Dl, J
A, Dl, J
A, F, J. K
A, C, G
A, C, G
A, F, G
A, F, G
A, F, G
A, F, G
A, J, J
A, F, J
A, F, J
A, F, J
A, F, G
A, F, G
A, F, G
A, F, G
A, F, G
A, F, G
A, C, G
A, C, G
A, F, H, L
A, F, J, K
A, F, J
A, F, J, K
A, F, J
A, F, J
A, F, J, K
A, F, J, K
A, F, J, K
A, F, J
A, F, J
A, F, G, K
A, F, J, K
A, F, J, K
* Letter codes are defined at end of table.
t Numbers in parentheses represent EPA sample numbers for used oil
samples obtained as part of their 1983 sampling program.
0306
A-146
-------
TABLE A-3 (continued)
USED OIL SAMPLE IDENTIFICATION CODES
SAMPLE
NUMBER
721
722
723
724
725
726
727
728
729
730
731
732
733
734
735
736
737
738
739
740
741
742
743
744
745
746
747
748
749
750
751
752
753
754
755
756
757
758
759
760
(195)t
(197)
(198)
(200)
(201)
(203)
(206)
(223)
(224)
(225)
(232)
(244)
(251)
(252)
(253)
(254)
(270)
CODE*
A,
A,
A,
A,
A,
A,
A,
A,
A,
A,
A,
A,
A,
A,
A,
A,
A,
F,
F,
F,
F,
F,
F,
F,
F,
F,
F,
F,
F,
F,
F,
F,
F,
F,
F,
F,
F,
F,
F,
F,
F,
F,
F,
F,
F,
F,
F,
F,
C,
F,
F,
E4
C,
Dl
Dl
F,
E3
J,
J,
J,
J,
J,
J,
J,
J,
J,
J,
J,
J,
J,
J,
J,
J,
J,
J,
J,
J,
J,
J,
J,
J, R
J, R
I, K
J, R
J
J, R
J, R
H, R
H, R
H, R
G, L
, J, R
J, R
, J, R
, J, R
J, R
, J, R
R
R
R
K
R
R -
L
L
R
K
R
R
L
L
L
L
R
K
R
K
K
L
L
SAMPLE
NUMBER
761
762
763
764
765
766
767
768
769
770
771
772
773
774
775
776
777
778
779
780
781
782
783
784
785
786
787
788
789
790
791
792
793
794
795
796
797
798
799
800
(333)
(348)
(354)
(356)
(1)
(2)
(3)
(4)
(5)
(6)
(10)
(51)
(52)
(62)
(63)
(64)
(65)
(66)
(67)
(92)
(93)
(94)
(122)
(297)
(320)
(326)
(327)
(328)
(329)
CODE
F,
F,
F.
F,
F,
F,
F,
F,
F,
F,
F,
A,
A,
A,
A,
A,
A,
A,
A,
A,
A,
A,
A,
A,
A,
A,
A,
A,
A,
A,
A,
A,
A,
A,
A,
A,
A,
A,
A,
A,
J,
J,
J,
J,
J,
J,
J,
J,
J,
J,
J,
F,
B,
F,
B,
F,
F,
F,
F,
F,
F,
D4
DA
D3
F,
F,
F,
F,
F,
F,
E3
F,
C,
C,
F,
F,
C,
C,
F,
C,
L
L
R
R
R
R
R
R
R
R
R
J
H,
J,
J,
J
J
J
J
J
J
, J
» J
» J
G
G
G
G
G
G
, J
G
J,
J,
J
G
G
G
G
G
R
R
R
, R
, R
R
R
* Letter codes are defined at end of table.
t Numbers in parentheses represent EPA sample numbers for used oil
samples obtained as part of their 1983 sampling program.
A-147
-------
TABLE A-3 (continued)
USED OIL SAMPLE IDENTIFICATION CODES
-_====
SAMPLE
NUMBER
801 (335)t
802 (337)
803 (338)
804 (339)
805 (340)
806 (341)
807 (342)
808 (343)
809 (344)
810 (345)
811 (359)
812 (360)
813 (89)
814 (90)
815 (91)
816 (95)
817 (96)
818 (98)
819 (99)
820 (101)
821 (102)
822 (103)
823 (214)
824 (216)
825 (217)
826 (226)
827 (227)
828 (234)
829 (235)
.830 (236)
831 (237)
832 (238)
833 (240)
834 (275)
835 (276)
836 (278)
837 (279)
838 (331)
839 (332)
840
CODE*
A, F, G
A, F, G
A, F, G
A, F, G
A, C, G
A, C, G
A, C, G
A, C, G
A, C, G
A, C, G
A, F, J
A, F, J
A, F, G
A, F, G
A, F, J
A, F, J, K
A, F, J, L
A, F, G, K
A, F, J, K
A, F, J, K
A, F, G, K
A, F, J, L
A, F, J, L
A, F, J, L-
A, F, J, K
A, El, J
A, Dl, J, K
A, F, G, K
A, Dl, J, K
A, Dl, J, K
A, F, G, K
A, Dl, J
A, Dl, J, K
A, D2, J
A, D2, J, K
A, D2, J
A, F, J
A, F, J
A, F, J
B, J
SAMPLE
NUMBER
841
842
843
844
845
846
847
848
849
850
851
852
853
854
855
856
857
858
859
860
861
862
863
864
865
866
867
868
869
870
871
872
873
874
875
876
877
878
879
880
CODE
B, J
B, J
B, J
B, J
B, J
B, J
B, J
B, J
B, J
B, J
B, J
B, J
B, J
B, J
B, J
B, J
B, J
B, J
B, J
B, J
B, J
B, J
B, J
B, J
B, J
B, J
B, J
B, J
B, J
B, J
B, J
B, J
B, J
B, J
B, J
B, J
B, J
B, J
B, J
C. J, K
* Letter codes are defined at end of table.
f Numbers in parentheses represent EPA sample numbers for used oil
samples obtained as part of their 1983 sampling program. 0307
A-148
-------
TABLE A-3 (continued)
USED OIL SAMPLE IDENTIFICATION CODES
SAMPLE
NUMBER
881
882
883
884
885
886
887
888
889
890
891
892
893
894
895
896 .
897
898
899
900
901
902
903
904
905
906
907
908
909
910
911
912
913
914
915
916
917
918
919
920
CODE*
C, J, R
C, J, R
C, J, K
C, J, K
C, J, L
C, J, L
C, J, K
C, J, R
C, J, R
C, J, K
C, J, K
C, J, K
C, J, K
C, J, K
C, J, K
C, H, K
C, H, K
E4, G, L
E4, G, L
E4, G, L
E4, G, L
E4, G, L *
E4, G, L
E4, G, L
E4, G, L
E4, G, L
E4, G, L
E4, G, L
E4, G, L
E4, G, K
E4, G, K
E4, G, K
E4, G, K
E4, G, R
E4, G, K
E4, G, K
E4, G, K
E4, G, K
E4, G, K
E4, G, K
SAMPLE
NUMBER
921
922
923
924
925
926
927
928
929
930
931
932
933
934
935
936
937
938
939
940
941
942
943
944
945
946
947
948
949
950
951
952
953
954
955
956
957
958
959
960
CODE
E4, G, L
E4, G, L
E4, G, L
E4, G, L
E4, G, R
E4, G, R
E4, G, R
E4, G, R
E4, G, R
E4, G, R
E4, G, R
E4, G, R
E4, G, K
£4, G, R
E4, G, R
£4, G, R
E4, H, L
E4, H, L
E4, H, R
E4, H, R
E4, H, R
E4, H, R
E4, H, R
E4, H, R
E4, H, R
E4, H, R
E4, H, R
F, I, R
F, I, R
F, I, R
F, I, R
F, I, R
F, I, R
F, I, R
F, I, R
F, I, R
F, I, R
F, I, R
F, I, R
F, I, R
* Letter codes are defined at end of table.
A-149
-------
TABLE A-3 (continued)
USED OIL SAMPLE IDENTIFICATION CODES
SAMPLE
NUMBER
961
962
963
964
965
966
967
968
969
970
971
972
973
974
975
976
977
978
979
980
981
982
983
984
985
986
987
988
989
990
991
992
993
994
995
996
997
998
999
1000
CODE*
F, I, K
F, I, K
F, I, K
F, H, K
F, H, K
F, H, K
F, H, K
F, H, K
F, H, K
F, H, K
F, H, K
F, H, K
F, H, K
F, Q, K
F, Q, K
F, Q, K
F, Q, K
F, Q, K
F, Q, K
F, Q, K
F, Q, K
F, Q, K
F, Q, K
F, Q, K
F, Q, K .
F, Q, K
F, Q, K
F, Q, K
F, Q, K
F, Q, K
F, Q, K
F, Q, K
F, Q, K
F, Q, K
F, Q, K
F, Q, K
F, Q, K
F, J, L
F, J, L
F, J, K
SAMPLE
NUMBER
1001
1002
1003
1004
1005
1006
1007
1008
1009
1010
1011
1012
1013
1014
1015
1016
1017
1018
1019
1020
1021
1022
1023
1024
1025
1026
1027
1028
1029
1030
1031
1032
1033
1034
1035
1036
1037
1038
1039
1040
CODE
F, J, K
F, J, K
F, J, K
F, J, L
F, J, L
F, J, K
F, J, K
F, J, K
F, J, K
F, J, K
F, P, L
F, P, L
F, P, L
F, P, L
F, P, L
F, P, L
F, P, L
F, P, L
F, P, L
F, P, L
F, P, L
F, P, L
F, P, L
F, P, L
F, P
F, P, K
F, P, K
F, P, K
F, P, K
F, P, K
F, P, K
F, P, K
F, P, K
F, P, K
F, P, K
F, P, K
F, P, K
F, P, K
F, J, L
F, J, L
* Letter codes are defined at end of table.
0308
-------
TABLE A-3 (continued)
USED OIL SAMPLE IDENTIFICATION CODES
SAMPLE
NUMBER
1041
1042
1043
1044
1045
1046
1047
1048
1049
1050
1051
1052
1053
1054
1055
1056 (80) t
1057 (81)
1058 (82)
1059 (83}
1060 (84)
1061 (85)
1062 (86)
1063 (358)
1064 (361)
1065 (306)
1066 (34)
1067 (36)
1068 (37)
1069 (50)
1070 (54)
1071 (59)
SAMPLE
CODE* NUMBER CODE
F, J, L
F, J, L
F, J, L
F, J, L
F, J, L
F, J, L
F, J, L
F, J, L
F, J, L
F, J, L
F, J, L
F, J, L
F, J, K
F, J, K
F, J, K
A, F, G
A, F, G
A, F, G
A, F, G
A, F, G
A, F, G
A, C, J
A, J, J
A, F, J -
A, F, J
A, El, J
A, El, J
A, El, J
A, E4, J
A, E4, J
A, E4, J
* Letter codes are defined at end of table.
t Numbers in. parentheses represent EPA sample numbers for used oil
samples obtained as part of their 1983 sampling program.
A-151
-------
TABLE A-3 (continued)
USED OIL SAMPLE IDENTIFICATION CODES
SAMPLE CODE KEY
A - Sample analyzed as part of EPA's 1983 used oil sample program
8 - Automotive oil; sample taken from generator
C - Automotive oil; sample taken from collector or processor
D - Industrial oil; sample taken from generator
Dl - Cutting or machine oils
D2 - Cooling oils
D3 - Hydraulic oils
D4 - Unknown oil types
E - Industrial oil; sample taken from collector or processor
El - Cutting or machine oils
E2 - Cooling oils
E3 - Hydraulic oils
E4 - Unknown oil types
F - Unknown oil source
G - Burned as fuel
H - Re-refined
I - Road oil
J - Unknown end-use
P - Road oil or burned as fuel
Q - Road oil or re-refined
A-152
0300
-------
-------
APPENDIX A
REFERENCES
A-l Unpublished analytical data obtained from the office of
Norman F. Surprenant, GCA Corporation, Inc., Bedford,
Massachusetts, July 1982.
A-2 U.S. Environmental Protection Agency. Assessment of indus-
trial hazardous waste management, petroleum re-refining
industry. 1977.
A-3 Reindl, J. Waste oil recycling. Journal of Environmental
Health, Vol. 40, No. 1, July/August 1977, pp. 52-55.
A-4 Linnard, R. £., and L. M. Henton. Re-refined waste oil with
PROP. Hydrocarbon Processing, September 1979, pp. 148-153.
A-5 Unpublished analytical data obtained from Thomas Manning,
Resource Technology, Inc., June 1982.
A-6 Bartlesville Energy Research Center. Waste lubricating oil
research: A comprehensive characterization of five typical
re-refinery feedstocks, Part 5. April 1977.
A-7 Stephens, R. D., et al. A study of the fate of selected
toxic materials in waste oils used for dust palliation on
logging roads in the Plumas National Forest. California
Department of Health Services. March 1981.
A-8 Unpublished analytical data obtained from Henry Aho, Maine
Department of Environmental Protection, July 6, 1982.
A-9 Nims, J., et al. An analysis of waste oil in Maine. Maine
Department of Environmental Protection. 1981.
A-10 Smith, I. C., T. L. Ferguson, and B. L. Carson. Metals in
new and used petroleum products and by-products. Midwest
Research Institute. Not dated.
A-ll Hess, L. Y. Reprocessing and disposal of waste petroleum
oils. NOYES Data Corporation, Park Ridge, New Jersey.
1979.
0310
A-153
-------
A-12 Raymond, R. L., J. O. Hudson, and V. W. Jamison. Oil degra-
dation in soil. Applied and Environmental Microbiology,
April 1976, pp. 522-535.
A-13 Freestone, F. J. Runoff of oils from rural roads treated to
suppress dust. U.S. Environmental Protection Agency.
Publication EPA-R2-72-054, October 1972.
A-14 Winters, K., and P. L. Parker. Water soluble components of
crude oils, fuel oils, and used crank-case oils. Proceed-
ings; 1977 Oil Spill Conference (Prevention, Behavior, Con-
trol, Cleanup), March 8-10, 1977, New Orleans, pp. 579-581.
A-15 Cotton, F. 0., et al. Analysis of 30 used motor oils.
Hydrocarbon Processing, September 1977, pp. 131-140.
A-16 Geyer, C., and E. Glendening. The used oil recycling program
Oregon Department of Environmental Quality. Not dated.
A-17 May, W. E., and J. M. Brown. The analysis of some residual
fuel and waste lubricating oils by a high-performance liquid
chronatographic procedure. Proceedings? Workshop on Measure-
ments and Standards for Recycled Oil, NBS, Gaithersburg,
Maryland, November 29-30, 1977. Issued September 1979.
A-18 Coyle, T. D., and A. R. Siedle. Metals in oil: Occurrence
and significance for reuse of spent automotive lubricating
oils. Proceedings? Workshop on Measurements and Standards
for Recycled Oil, NBS, Gaithersburg, Maryland, November
29-30, 1977.
A-19 Yates, J. J., and K~. G. Croke. Used oil recycling in
Illinois Data Book. Prepared for the Illinois Institute of
Natural Resources by ETA Engineering, October 1978. Data
represents industrial samples obtained from Borg-Warner,
General Electric, Olin Brass, and John Deere.
A-20 Analytical data obtained from Tomas Leep, Water Quality
Division, Michigan Department of Natural Resources? analyse
performed over the period 1979 to 1981.
A-21 Analytical data obtained from Edgar J. Crowley, Division of
Air Quality, Minnesota Pollution Control Agency? date of
analysis 8-25-82.
A-22 Maney, J. P., N. Luedtke, and S. Drew. Hazardous waste
identification and listing support contract No. 68-01-6467,
delisting verification. Prepared by Energy Resources Co.,
Inc., for the U.S. Environmental Protection Agency. Sep-
tember 9, 1982.
A-154
-------
A-23 Massachusetts Department of Air Quality, Waste Oil Sampling
Program. Winter 1981/82, samples from facilities burning
waste oil.
A-24 Yates, J. J., and K. G. Croke. Used oil recycling in
Illinois Data Book. Prepared for the Illinois Institute of
Natural Resources by ETA Engineering, October 1978.
A-25 Swain, J. W. Industrial oils used as fuel. NBS Special
Publication 556. Proceedings; Workshop on Measurements and
Standards for Recycled Oil - II, Gaithersburg, Maryland,
November 29-30, 1977. p. 69.
A-26 Spawn, P. D., and P. F. Fennelly. An updated look at the
fuel potential of waste automotive oil. NBS Special Publi-
cation 556. Proceedings; Workshop on Measurements and
Standards for Recycled Oil - II, Gaithersburg, Maryland,
November 29-30, 1977. p. 51.
A-27 Linnard, R. E. Phillips recycled oil program. NBS Special
Publication 556. Proceedings; Workshop on Measurements and
Standards for Recycled Oil - II, Gaithersburg, Maryland,
November 29-30, 1977. p. 134.
A-28 Whisman, M. L., J. W. Goetzinger, and F. 0. Cotton. Waste
lubricating oil research. U.S. Bureau of Mines Pollution
RI 7925 (1974).
A-29 Skinner, D. J. Preliminary review of used oils in Canada.
Water Pollution Control Directorate. Report EPS 3-WP-74-4,
June 1974. Revised J,une 1976. p. 103.
A-30 Williams, B. R. Automotive crankcase drainings used for
fuel. NBS Special Publication 488. Proceedings; Workshop
on Measurements and Standards for Recycled Oil - II,
Gaithersburg, Maryland, November 22-23, 1976.
A-31 Unpublished data obtained from the Oklahoma Department of
Health; date of analysis: 9-4-80. Waste industrial oils to
be used for road base material.
A-32 Becker, D. A., and J. J. Comeford. Recycled oil program:
Phase I - test procedures for recycled oil used as burner
fuel. NBS Technical Note 1130, August 1980. p. 5.
A-33 Benz(a)pyrene concentration was given on page 51 of Refer-
ence A-32 for 11 used automotive oil samples and 8 used oil
samples taken from re-refiners' feedstocks. In ppm, the
automotive samples had concentrations of 10, 8, 11, 10, 11,
14, 14, 16, 12, 14, and 17; the re-refiners' feedstocks had
concentrations of 16, 10, 14, 13, 10, 14, 12, and 11.
0311
A-155
-------
A-34 Hazelwood, D. L., and F. J. Smith. Assessment of waste fuel
use in cement kilns. Prepared for Industrial Research Labo-
ratory, U.S. Environmental Protection Agency. March 1981.
A-35 Fu, T. T., and R. S. Chapler. Waste-oil boiler firing
demonstration at NAS Miramar, San Diego, California. Pre-
pared by Naval Civil Engineering Laboratory, Port Hueneme,
California. January 1982. p. 12.
A-36 Stringer, P. L. Correlation aspects of a virgin and a
re-refined engine oil containing the same additives. Pre-
sented at the NBS Conference on Measurements and Standards
for Recycled Oil - IV, September 12-16, 1982, Gaithersburg,
Maryland.
A-37 Weinstein, N. J. Waste oil recycling and disposal. Pre-
pared by Recon Systems, Inc., for the U.S. Environmental
Protection Agency. August 1974. p. 12.
A-38 Frame, E. A., and T. C. Bowen. U.S. Army/Environmental
Protection Agency re-refined engine oil program. AFLRL
Report No. 98, May 1978.
A-39 Unpublished analytical data obtained from the U.S. Environ-
mental Protection Agency; received 12-21-82. Data represent
automotive crankcase oil samples used as fuel.
A-40 Cheng, S. C., et al. Alternative treatment of organic
solvents and sludges from metal finishing operations.
Monsanto Research Corporation for the U.S. Environmental
Protection Agency. January 15, 1982. (Draft report.)
A-41 University of Wisconsin - Extension. Waste motor oil in
Wisconsin - A neglected resource. June 1976.
A-42 Unpublished data obtained from the U.S. Environmental Pro-
tection Agency; received 1-3-82. Data represent samples
taken from waste oil collectors in Connecticut. All oil
collected is assumed to be sold as fuel.
A-43 Unpublished composition data obtained from John R. Purvis,
New Jersey Department of Environmental Protection, September
3, 1982.
A-44 Unpublished composition data obtained from Wallace E.
Sonntag, Engineer with the New York State Department of
Environmental Conservation, January 11, 1983.
A-45 Unpublished composition data obtained from John R. Purvis,
New Jersey Department of Environmental Protection, January
7, 1983.
A-156
-------
A-46 GCA Corporation, "The Fate of Hazardous and Nonhazardous
Wastes in Used Oil Recycling," Fifth Quarterly Progress
Report, DOE DE-AC19-81BC10375, March 15, 1983.
A-47 Kansas City Star, Sunday, December 26, 1982 p. 25A.-
A-48 Unpublished analytical data developed for the Office of
Solid Waste, U.S. EPA by ERCO, 1983.
A-49 Unpublished analytical data developed by the National
Enforcement Investigation Center, U.S. EPA, 1983.
A-50 Ulrichson, D., and Yake, D. Iowa Re-refined Oil Fleet Test.
Engineering Research Institute, Iowa State University, Anies,
Iowa. October 1978.
A-157
0312
-------
-------
Appendix B
DATA BASE FOR
CONTAMINATION OF RESIDUES FROM
WASTE OIL PROCESSING AND RE-REFINING
0313
B-l
-------
TABLE B-l
METALS CONCENTRATIONS IN SETTLED SLUDGES
GENERATED DURING WASTE OIL STORAGE AND PROCESSING a/
Arsenic
<5
<5
<5
<1
<5
<5
<5
<5
r<5 b/
L 5 I/
<5
<5
r<5b/
L 17 c/
24 b/
<5 ~
<5
<5
<5
12
<5
12
14
<5
<5
5
r <5 b/
L <5 I/
0.013
<5
<5
<5
<5
<5
<5
<5
<5
<5
21
12
-
-
-
_
-
-
-
_
Barium
38
19
18
70
70
90
30
80
50
<10
47
4«
19
28
f 25 b/
L 1,950 c/
[1,200 b/
21 I/
3,610 c/
r 102 ₯/
L 385 I/
56 b/
310
420
<50
210
20
66
131
64
33
830
1.300
f 916 b/
L 1,140 c/
0.21
27
748
2,590
280
<50
<50
90
220
270
110
180
-
_
Cadmium
<0.5
<0.5
<0.5
<7
<7
<7
<7
r /
L <5 ^/
<5 b
<7
<7
<7
^10
^10
6
<5
<5
47
48
rso b/
L 47 c/
0.02
<8
148
11
*^10
*^10
^10
^10
<1Q
-------
TABLE B-2
TOTAL CHLORINE AND CHLORINATED SOLVENTS CONCENTRATIONS
IK SETTLED SLUDGES GENERATED DURING WASTE OIL STORAGE AND PROCESSING a/
Dichlorodifluoromethane
1.1.1-
Trichloroethylene
Trichloroethylene Tetrachloroethylene Total Chlorine
<1
<10
1.3
59
22
34
30
640
19
190
570
7,500
120
86
640
260
2,200
300
300
<100
1.200
<100 b/
110,000 b/
5,100 b/
420
9,900
790
5,400
<100
1,300
1,100
300
<100
500
400
200
<100
<100
<100
<200
2,300
-<200
240
<200
430
<100
770
2.2
5.7
1,300
360
37
110
370
730
600
100
<100
1,100
<100
900
1,100
<100 b/
900 b/
1,100 b/
<100
310
130
190
<100
<100
100
<100
<100
<100
<100
200
<100
<100
<100
<200
<200
<200
2.200
<200
<200
<100
<100
70
580
1,900
111
210
130
830
1.000
1.500
<100
1,600
1,000
1.500
<100
1.600
100 b/
1,400 b/
7.000 b/
740
210
200
210
<100
2.400
800
8,200
<100
<100
300
<100
<100
<100
<100
<200
<200
<200
<200
<200
<200
<100
<100
4,700
1.500
1.200
13,300
8,960
740
13.100
f 746 b/
I 2,940 c/
[2,530 b/
933 d/
1,880 c/
r 181,000 b/
I 75.400 c/
7,790 b/
2,910
3,630
88
2.390
1,300
5.080
2.540
13,600
220
1.860
1.540
1.470
2,110
593
1,270
851
1,780
1.300
<200
1,370
610
718
3,950
1,120
£/ All data are presented in ppm. No data were available on trichlorotrifluoroethane concentration.
b/ A top layer phase of an oily sludge residue.
c/ A bottom layer phase of an oily sludge residue.
~ZJ A middle layer phase of an oily sludge residue.
Note: Data for samples from different layers of the same storage tank are grouped.
Source: References B-24 to B-31.
0314
B-3
-------
TABLE B-3
OTHER ORGANICS CONCENTRATIONS
IN SETTLED SLUDGES GENERATED DURING
WASTE OIL STORAGE AND PROCESSING a/
PCBs Benzo(a)pyrene Phenol
1.4
<50 2.0 <1
<50 <1 <1
<50 <1 <1
<50 3.6 5.5
<10 12 11
<50 1.4 2.4
<4 16
28
<1
17
<1
<5
<10
500
<50
<50
<50
<50
<50
<50
<50
<50
<50
<50
<50
<2
<50
<50
a/ All data are presented in ppm. No data were available for the concen
tration of benzene, toluene, xylene, benzo(a)anthracene, or naphthale
Source: References B-24 to B-31.
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-------
TABLE B-6
OTHER ORGANICS CONCENTRATIONS IN WASTEWATER
GENERATED DURING WASTE OIL STORAGE AND PROCESSING a/
Benzene
<0.4*
<20*
550
38
24
150
890
290
300
669
Benzo(a)-
Toluene anthracene
14* <1*
1,300* <0.02*
840
120
2,500
530
5,800
640
630
693
Benzo(a)-
pyrene Naphthalene
<1* <1*
<0.02* 0.7*
ND b/
120
ND
700
470
ND
180
229
PCBs
<1*
<10*
<0.04*
14*
<0.04*
0.1*
<0.04*
<0.04*
<0.04*
<0.04*
<0.04*
Pheno:
65
<1*
0.02'
6,000
4,600
99,000
15,000
48,000
19,000
5,100
2,800
0.2*
<0.04*
<0.04*
0.04*
0.19*
<0.04*
ND
ND
ND
ND
ND
ND
ND
ND
ND
<10*
<10*
<5*
All data are reported in mg/£. unless coded by an (*) in which case the unit of measure-
ment is ppm. No samples were analyzed for xylene.
Not detected, however, no detection limit was reported.
irce: References B-20, B-22, B-24, B-26, B-27, and B-31.
031G
B-7
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-------
TABLE B-8
CONCENTRATION OF POTENTIALLY HAZARDOUS CONSTITUENTS
IN DISTILLATION BOTTOMS FROM RE-REFINING FACILITIES a/
Sample Number
etals
Arsenic
Barium
Cadmium
Chromium
Lead
Zinc
-
1,400
0
100
15,000
3,500
8.3
14
5.7
35
2,090
2,960
<0.01
25
20
7
1,090
126
1.0
6
9
11
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85
15
940
29
63
10,300
133
hlorinated Solvents
Dichlorodifluoromethane - b/ - - - -
Trichlorotrifluoroethane - - - -
1,1,1-Trichloroethane -
Trichloroethylene -
Tetrachloroethylene -
Total Chlorine -
ther Organics
Benzene -
Toluene _----.
Xylene - - ' -
Benzo(a)anthracene - <4 - - -
Benzo(a)pyrene - <4 - - -
Naphthalene - - <4
PCBs - <11
eference B-7 B-22 B-26 B-26 B-26
/ All values are reported in ppm.
/ (-) indicates constituent was not measured. Generally, distillation bottoms are belie\
to contain very low levels of chlorinated and organic solvents.
0317
B-9
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B-10
-------
Appendix B
REFERENCES
B-l. Jervis, R.E. Trace Impurities in Canadian Oil Sands, Coals and
Petroleum Products and Their Fate During Extraction, Up-Grading,
and Combustion. Journal of Radioanalytical Chemistry, 71, No.
1-2. 1982. pp 225-241.
B-2. Unpublished data obtained by David William (U.S. EPA) from Steven T.
Cragg (American Petroleum Institute). August 19, 1982.
B-3. U.S. Environmental Protection Agency. Environmental Assessment of
Residual Oil Utilization - Second Annual Report. September 1978.
EPA 600/7-78-175.
B-4. Electric Power Research Institute. Study of Electrostatic Precipi-
tators Installed on On-Fired Boilers, Volume II. June 1978.
B-5. U.S. Environmental Protection Agency. Listing Waste Oil as a Hazardous
Waste. Report to Congress (SW-909). January 16, 1981.
B-6. Mascetti, G.J. and H.M. White. Utilization of Used Oil. Prepared for
the U.S. Department of Energy by the Aerospace Corporation. August
1978.
B-7. Becker, D.A., Editor. Measurements and Standards for Recycled Oil -
II. NBS Conference Proceedings, November 29-30, 1977.
B-8. Unpublished data obtained from John R. Purves, Office of Regulatory
Services, New Jersey Department of Environmental Protection. Jan-
uary 7, 1983.
B-9. Unpublished data obtained from Wallace E. Sonntag, New York State
Department of Environmental Conservation. January 11, 1983.
B-10. Hall, Robert R. Comparative Analysis of Contaminated Heating Oils.
Prepared for the U.S. Environmental Protection Agency by GCA Cor-
poration. May 1983.
B-ll. Unpublished data. U.S. Environmental Protection Agency Files. No
date.
B-12. Unpublished data received from Motor Oils Refining Company, McCook,
Illinois. No date.
B-13. Yen, T.F. The Role of Trace Metals in Petroleum. Ann Arbor Science
Publishers. Ann Arbor, Michigan. 1975.
0318
B-ll
-------
B-14. Valkovic, Vlado. Trace Elements in Petroleum. Petroleum Publishing
Company. 1980.
B-15. McCoy, J. The Inorganic Analysis of Petroleum. Chemical Publishing
Company. New York. 1962.
B-16. Proceedings of Symposium on Nonhydrocarbon Constituents of Petroleum.
Milwaukee, Wisconsin. March 30-April 3, 1952.
B-17. Bell, J.D. Recycling of Used Lubricating Oil as a Dust Suppressant,
Review of Current Knowledge and Recommendations for Further Investi-
gations. Prepared for the Petroleum Association for Conservation of
the Canadian Environment. December 1976.
B-18. Zobeli, C.E. Sources and Biodegradation of Carcinogenic Hydrocarbons
Proceedings of Joint Conference on Prevention and Control of Oil Pol-
lution. 1971.
B-19. Department of Energy. Motor Gasoline, Winter 1979-80. (DOE/BETC/
PPS-80/3). July 1980.
Residuals
B-20. Stoll, J.W. Wastewater Treatment System Design for the Re-refining
Industry. Proceedings of the Fourth International Conference on
Used Oil Recovery and Reuse. Association of Petroleum Re-refiners.
September 28-October 1, 1981.
B-21. Swain, J.W. Assessment of Industrial Hazardous Waste Management
Practices, Petroleum Re-refining Industry (SIC 2992). U.S. Environ-
mental Protection Agency. September 1976.
B-22. GCA Corporation. The Fate of Hazardous and Nonhazardous Wastes in
Used Oil Recycling. Prepared for Bartlesville Energy Technology
Center, Department of Energy. April 15, 1983.
B-23. Confidential data obtained by Franklin Associates, Ltd. included in
an environmental impact statement for a waste oil processing facili
Received March 1983.
B-24. Unpublished data obtained from John R. Purves, New Jersey Departmen
of Environmental Protection. September 3, 1982.
B-25. Unpublished data obtained from Don Hensh, Oklahoma State Department
of Health, November 4, 1982. Material is waste oil sludge mixed wi
rock used as a road base material.
B-26. Weinstein, K.D., T.D. Meyers, and S.R. Craft. Enhanced Utilizatiot
of Used Lubricating Oil Recycling Process By-Products. Prepared b}
Booz, Allen & Hamilton, Inc. for the U.S. Department of Energy (BE:
DOE/BC/10059-19. March 1982.
B-12
-------
B-27. Confidential data developed by the U.S. Environmental Protection
Agency, National Enforcement Investigations Center, obtained sum-
mer and fall, 1983.
B-28. Nims, J., et al. An Analysis of Waste Oil in Maine. Maine Depart-
ment of Environmental Protection. 1981.
B-29. Unpublished analytical data obtained from Henry Aho, Maine Depart-
ment of Environmental Protection. July 6, 1982.
B-30. Unpublished data obtained from the U.S. Environmental Protection
Agency; received 1-3-83. Data represent samples taken from waste
oil collectors in Connecticut.
B-31. U.S. Environmental Protection Agency. Data developed by ERGO for
the Waste Characterization Branch, Office of Solid Waste. Summer/
Fall 1983.
0319
B-13
-------
Appendix C
METHODOLOGY AND REFERENCES FOR USED OIL FLOW DESCRIPTION
The flow of used oil through the UOMS was developed for 1983
using information obtained from many sources and through making several
assumptions based upon the best available information. This appendix
provides the references and assumptions used to develop each number in
the overall flow description.
Figure C-l shows the actual flow of oil through the UOMS In
millions of gallons. The volumetric data has been removed in Figure C-2
and letter codes have been substituted. The references and assumptions
used to develop each number in the flow are described below for each
letter code.
It is important to note that the methodology which is used
accounts for oil flow only. Contaminants which accumulate in oil such
as water and solids are not included in the volumetric estimates. There-
fore, the actual quantity of material which is handled is greater, per-
haps by 10 percent, than the quantities shown.
(a) In 1983, a total of 1,251 million gallons of
automotive lubricants were sold in the United
States (C-12). About 94 percent of these
oils were crankcase or hydraulic oils which
comprise most of the oils generated following
use. According to information obtained from
(C-12), 42.1 percent of these oils were con-
sumed in passenger cars and 15.5 percent in
light trucks. Approximately 9.5 percent of
these oils were hydraulic fluids. Triple A
reports that 80 percent of passenger cars
and 54 percent of light trucks are privately
owned. For privately owned vehicles, a DOE
study indicated that 64 percent of all oil
changes are carried out by do-it-yourselfers
(DIYers) (C-l). Finally, oil generation
factors for passenger cars and light trucks
are 0.68 and 0.63, respectively (only 0.10
for hydraulic fluids). Using this informa-
tion, the total quantity of used oil generated
by DIYers is calculated below:
Passenger cars
Crankcase - [1,251 x (.94) x (.421) x (.80)
x (.64) x (.68)] = 155.2
Hydraulic oil - [1,251 x (.94) x (.421) x (.10)
x (.80) x (.64) x (.10)] - 2.5
Subtotal 157.7
c-i 0320
FRANKLIN ASSOCIATES, LTD.
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§
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1 1
in
CM
c
o
o
ee
. j
CM
m
CVJ
f
a
i
sg
£tz»
^ cc m
§§*
5 = 1
192.3 million gal
use In on- site bo
bases, used oil p
I «/t t/i >>
i!.^
'o u
Iff1
C-2
-------
0321"
C-3
-------
Light Trucks
Craakcase - [1.251 x (.94) x (.155) x (.90)
x (.54) x (.64) x (.63) - 35.6
Hydraulic Oil - [1,251 x (.94) x (.155) x (.10)
x(.54) x (.64) x (.10) -
Subtotal
Total DIYer Oil 193.9
(b) The management of used oil generated by DIYers was assumed
to be equal to the average practices reported by DOE for
conditions in 1981 (C-l). Volumes managed in each way were
calculated from total generation using the following per-
centages:
Take to recycle center - 14.0 (27.1 mil gal)
Disposal - 21.0 (40.8 mil gal)
Dumping - 60.9 (118.0 mil gal)
Burning - 4.1 (8.0 mil gal)
100.0
(c) The total quantity of used oil generated at "automotive
generators" (see definition in Section 2.0) was calculated
based upon sales to certain markets. These markets include
personal and commercial vehicles with commercial being
either fleet or non-fleet. The generation by non-DIYer
personal vehicles can be calculated by using the same
method and equations as presented above for DIYers.
Oil generation by non-DIYer personal vehicles is about
55 percent of that generated by DIYers. or 106.8 million
gallons. Oil generation by commercial vehicles is cal-
culated below based upon sales (C-12) and generation
factors (C-.2) and (C-12) for three basic markets and
two general oil types.
, (Generation (Used Oil
(Sales - 10 gal) x Factor) - Generati
Passenger Cars
Crankcase (86.8)
Hydraulic (9.6)
Light Trucks
Crankcase (72.0)
Hydraulic (8.0)
Medium & Heavy Trucks & Buses
Crankcase (139.7)
Hydraulic ( 15.7)
x (0.68)
x (0.10)
Subtotal
x (0.63)
x (0.10)
Subtotal
x (0.59)
x (0.10)
Subtotal
60.0
82.42
1.57
84.0
Total - Commercial Vehicles 190.2
C-4
FRANKLIN ASSOCIATE
-------
The remaining automotive used oil generation results
from off-road engines including such uses as farming, con-
struction, mining, military, and aviation. Both crankcase
and hydraulic oil sales (C-12) and generation factors (C-2)
and (C-12) were used to calculate used oil generation in
these markets as shown below.
Off-Road Market
Farming
Crankcase
Hydraulic
, (Generation
(sales - 10 gal) x Factor)
(Used Oil
Generation;
(74.1)
(39.7)
x (0.59)
x (0.75)
Subtotal
Construction
Crankcase
Hydraulic
(68.8)
(34.7)
x (0.59)
x (0.75)
Subtotal
Mining
Crankcase
Hydraulic
(45.5)
(23.1)
x (0.59)
x (0.75)
Subtotal
Government
Crankcase
Hydraulic
(11.7)
( 6.3)
x (0.63)
x (0.75)
Subtotal
Aviation
Crankcase
Hydraulic
(12.7)
( 7.6)
x (0.47)
x (0.75)
Subtotal
Total - Off-Road Vehicles 208.1
The total volume of oil accumulated at automotive
generators equals the sum of the following components:
Oil received from DIYers -
Non-DIYer personal vehicles -
Commercial on-road vehicles -
Off-road vehicles -
Total
27.1 mil gal
106.8 mil gal
190.2 mil gal
208.1 mil gal
532.2 mil gal
C-5
FRANKLIN ASSOCIATES, LTD.
-------
(d) The letter "d" codes represent outputs from automotive
generators.
(dl) - Some automotive oils are generated by industrial
establishments due to the use of vehicle fleets.
This quantity was estimated assuming that 8 per-
cent of the oil generated by medium and heavy
trucks and buses is in industry fleets. This
percent is equal to the percent of total fleets
comprised by the manufacturing process and
petroleum industries (C-13).
(d2) - Automotive generators use their oil as fuel in
three major applications: (1) waste oil heaters;
(2) diesel engines; and (3) on-site boilers.
Some minor burning may take place in other fuel
applications, but that activity is not included
in this estimate.
Used oil heaters burn primarily automotive oils.
They are usually located at automotive generator
sites. It has been estimated that about 30,000
heaters are currently in use in the United States
with a typical rating of about 250,000 Btu/hour
(C-4). Based upon this rating and other information
received from industrial contacts, it was assumed
that a typical unit would burn 1,140 gallons per
year. The total quantity of used oil burned in this
way is estimated to be 34.2 million gallons in 1983.
Little documented information is available on used
oil combustion in diesel engines. Some large diesel
engine manufacturers, such as Cummins, have provided
customers with instructions and apparatus for blend-
ing used diesel oil with diesel fuel for burning in
diesel engines. The blending ratio is about 50 to
1 (fuel to oil). It is estimated that only 10 to
20 million gallons of the 200 plus million gallons
of truck oil is burned in this way. The midpoint
of 15 million gallons per year was assumed for this
study.
Burning of automotive oils in on-site boilers is
primarily limited to the U.S. Department of Defense
Approximately 50 percent of total generation by U.S
government installations (6.0 million gallons!, is
estimated to be burned on-site (C-14).
Overall. 55.2 million gallons (34.2 + 15 + 6.0)
of generated used automotive oil is estimated to be
burned directly by generators.
C-6
FRANKLIN ASSOCIATE
-------
(d3) - It was assumed that 20 percent of the used oil
generated by the farming, construction, and mining
industries which was not collected into the UOMS
was used to oil roads or other unpaved areas to
suppress dust or to provide an asphaltic effect
to the surface. Total non-collected generation
for these sectors was 125.3 million gallons in
1983. This volume equals 80 percent of farm
generation and 60 percent of construction and
mining generation. Twenty percent of this volume
equals 25.1 million gallons?
(d4) - Some generated used oil is dumped by non-fleet
commercial vehicle operators and a substantial
volume is dumped by operators of off-road vehicles.
Most dumping is simply allowing oil to drain from
a crankcase onto an unpaved lot or road; however,
it is sometimes collected and used in a haphazard
manner for other purposes such as weed or insect
control. It was assumed that 12.5 percent of all
oil generated by commercial vehicles is dumped.
This practice is only common for small non-fleet
situations where the volume of oil generated is
too small to warrant storage with subsequent col-
lection. The 12.5 percent estimate assumes 50
percent of the commercial vehicle oil generation
is for non-fleet vehicles (91.8 million gallons);
50 percent of that oil is not collected into the
TOMS (45.9 million gallons); and 50 percent of the
non-collected generation is dumped (22.9 million
gallons).
As stated in the preceding section, 125.3 million
gallons of used oil generated by the farming, con-
struction, and mining industries is not collected
into the UOMS. Of this total, 80 percent (or 100.2
million gallons) is believed to be dumped.
Overall, 123.2 million gallons of used automotive
oil is estimated to be dumped by generators, not
including DIYers.
(d5) - Only a small amount of generated used automotive
oil is believed to be disposed of through conven-
tional methods (e.g., sanitary landfill). It was
estimated that 10 percent of the non-collected, non-
fleet, commercial vehicle oil was managed in this
way:
Disposed oil - (45.9 mil gal) x (.10) » 4.6 mil gal
C-7
0321
FRANKLIN ASSOCIATES, LTD.
-------
(e) Total used oil generation by industrial establishments
was determined based upon sales reported in (C-12) and
generation factors reported in (C-2) and (C-8) with some
adjustments by FAL. Table C-l summarizes this calculation
procedure. Note that actual generation (shown in parenthe-
sis for some oils) is lower than the theoretical volumes
calculated from the factors. This is because some oils
which are sold do not complete their life cycle in the
year in which they are sold. In effect, there are more
of these oils in use each year.
(f) Used oil management practices by industrial facilities
was estimated by determining generation by major industrial
sectors and applying survey results on average management
methods to the volume for each sector. Table C-2 shows
industrial oil generation in 1983 by the major sectors.
Table C-3 shows estimates of how the generated oils are
managed in each major sector.
(g) The total oil entering the UOMS is the sum of that supplied
by automotive generators and industrial generators. Oil
entering UOMS - 317.4 + 351.7 - 669.1 mil gal.
(h) Although many independent collector companies exist, it
was assumed that they only collect 25 percent of the oil
accumulated by generators. The remaining 75 percent is
collected by processors and re-refiners. This 25/75 per-
cent breakdown was estimated based upon collection prac-
tices in many geographical regions as reported by col-
lectors and processors. These percentages were applied
to the total oil entering the UOMS to give the volume
handled by independent collectors and the volume collected
directly by processors and re-refiners.
Ind. Collectors - (669.1) x (.25) - 167.3 mil gal
Direct Collection
by Proc. and
Re-ref - (669.1) x (.75) - 501.8 mil gal
(i) The distribution of oil from independent collectors
companies was estimated based upon telephone interviews
and site visits with collectors and processors. Approxi-
mately 62 percent of the collected oil is delivered to
processors or re-refiners. The remainder is sold directly
to end-use applications including road oiling (14%), direc
fuel sales (9.5%), and virgin fuel oil dealers (9.5%), or
lost to disposal (5%).
C-8
FRANKLIN ASSOCIATE
-------
Table C-l
1983 INDUSTRIAL OIL SALES/GENERATION
UO6 gal)
Sales x Generation Factor I/
I. General Industrial Oils
A. Hydraulic
B. Gear
C. Other Specified
1. Turbine Circ.
2. Refrigeration
3. Way
A. Compressor
5. Rock Drill Air Tools
D. Other
Subtotal
II. Industrial Engine Oils
A. Railroad Diesel
B. Marine
C. Natural Gas
Subtotal
III. Metalworking Oils
A. Metal Removing
B. Metal Forming
C. Metal Treating
D. Metal Protecting
Subtotal
IV.
Process Oils
A. Elecmcal
B. White
C. Rubber
D. Other
Subtotal
INDUSTRIAL GREASE
TOTAL INDUSTRIAL LUBRICANTS
VI. Industry Fleet Oils
A. Automotive Oil
TOTAL OIL GENERATION BY INDUSTRIAL GENERATORS
264
33
78
6
5
4
3
28
421
57
49
38
144
85
47
19
12
163
76
56
64
102
298
1,026
35
1,061
11.2
.80
.60
.60
.33
.60
.60
.60
.73
.20
.50
.20
1.00
0.60
0.60
0.10
.90
.10
.10
.10
55.3
0
53.5
Generation
211.2 (200) 21
20.0 (19.6)
(295.1)
11.4
24.5
7.6
85.0
28.2
11.4
1.2
125.8
68.4 (20.5) 3/
5.6
6.4
10.2
90.6 (42.7)
567.6 (507.1)
0
567.6 (507.1)
_!/ Generator factor equals the fraction available for collection into the used oil management system;
it does not include oil which ends up in wastewater treatment sludges generated on-site.
y Values in parentheses equal actual industrial oil generation Assuming that all oil sold in any one
~ year does not finish its life cycle in that same year. Thus, there is an accumulation of oil in
use in our industrial/conmercial system.
_3/ The relatively low level of actual used electrical oil generation is due to the fact that much of
~ electrical oil sales are to replace PCB oils in transformers. The generation of these PCB oils is
not included in this value since these oils do not enter the UOMS.
Source: Sales data: (C-12).
Generation factors: (C-2) and (C-8) and Franklin Associates, Ltd.
C-9
0323
-------
Table C-2
INDUSTRIAL OIL GENERATION - 1983
Number of Establishments
SIC
Major Generators
Less than
20
Employees
24 Wood Products 29,032
25 Furniture & Fixtures 6,128
26* I/ Pulp/Paper 72
27* Newspapers 7,745
28 Chemicals 2.179
30* Rubber/Plastic 6,673
31* Leather 206
32* Glass 237
33 Primary Metals 3,687
34 Fabricated Metals 20,985
35 Machinery 39,784
36 Electronics 9,785
37 Motor Vehicles 5,656
38 Instruments 5,145
39 Miscellaneous Manufacture 12,210
49* Electric Utilities -
Subtotal - Major Generators 149,524
All Other Mfg. Industries
Marine Terminals
Military
Commercial
Railroads
Sia^ior.ary Natural Gas Engines
Other Miscellaneous Uses _5/ *
Total Industrial Oil
Greater
than 20
Employees
Used Oil Generation
(103 gallons)
Total
Small
facilities
Large
Facilities
Total
5,451
3,450
548
2,475
1.880
5,127
170
228
3,966
12,791
14,234
7,329
3,430
1,988
3,556
1,068 2/
67,721
34,483
9,608
620
10,220
4.059
11,800
376
465
7,653
33,776
54,018
17, 114
9,086
7,133
15.766
1,068
217,245
2.908.7
135.0
30.1
US. 5
1,663.0
1.315.1
16.4
42.0
4.425.0
3,725.0
9,780.0
1.314.5
7,486.8
86.6
2,613.4
-
35,660.1
4,166.2
506.8
7,996.8
308.9
24.627.8
6,113.5
85.9
1.206.7
66,329.1
16.886.4
41,812.6
20,775.6
143,885.0
1.124.9
3,101.4
13,243.2
352,170.8
7.074.9
641.8
8.026.9
427.4
26.290.8
7,428.6
102.3
1.248. 7
70,754.5
20.611.4
51,592.6
22,090.1
151,371.8
1,211.4
5,714.8
13,243.2
387,830.9
140.000
153
153
NA.3/ -
NA
NA.
306
36.663.1
306
20,000 4?
11,400
7,600
50,000
513,800
I/*: The entire industry is not included in the major generator analysis because of a lack of data or be
~ segments are insignificant generators.
2/ All power plants in SIC 49 are assumed to satisfy the large establishment definition of >20 employe
_3/ NA: Not Available.
-_, Estimated from the total generation believed to be 24 million gallons.
5_/ Includes such things as the use of industrial oils in homes, commercial establishments, off-road
~ vehicles, etc.
Source: Franklin Associates, Ltd., from data provided in (C-9) to (C-ll) and (C-15).
C-10
-------
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0325
-------
(j) The total volume of used oil handled by reprocessors
and re-refiners is equal to the sume of that delivered
by independent collector companies (103.4 million
gallons) and that which is directly collected by pro-
cessor and re-refiner route trucks (501.8 million gal-
lons). The total input to these companies equals the
sum of these numbers or 605.2 million gallons.
(k) The distribution of collected used oil to the eight
selected model facilities is based upon several as-
sumptions. First, it should be emphasized that there
are actually many more types of facilities than the
selected typical models, and therefore, the total
volume of oil was "force fed" to a workable number of
facilities.
Three basic data sources were used to estimate oil
distribution to the typical models(1) the volume
handled per year by each model, (2) the total number
of processing and re-refining companies, and (3) the
total volume of oil delivered to these companies.
It has been reported that there are approximately 250
operating processors and re-refiners in the United
States (C-5). Some information is available through
limited surveys as to the number of specific company
types. Good information is available characterizing
the relatively small number of operating re-refiners.
Using available information, a series of iterations
was performed to determine a reasonable number of
facility types while maintaining the desired volume
of material throughput. Table C-4 shows the results
of those iterations and the estimated flows. The data
in Table C-4 are presented in two basic parts; one part
consisting of the first four columns and the second
part, the last column. The first part develops the
total annual volume and percent of oil passing through
each selected model type. The resultant estimates
yield a total volume which is greater than the actual
input to the model facilities (663 compared to 605.2
million gallons). This exercise was carried out to
determine the percentages shown in column four which
could be applied to the total input to processor
companies to give material flows into each model which
are consistent with the overall flow description. These
percentages were multiplied times the remaining input
material after the re-refiner volume of 85 million gal-
lons had been subtracted. This independent estimate of
re-refining was maintained because considerably more
information was available about this entire industry.
C-12
FRANKLIN ASSOCIATE:
-------
Table C-4
DEVELOPMENT OF BEST ESTIMATES OF USED OIL DISTRIBUTION HTTP PROCESSING ASP RE-REFINING MODELS
Model Facility
Minor Processors
MP-1
MP-2
Major Processors
MJP-1
MJP-2
MJP-3
MJP-4
Subcocal - Processing
Re-Refiners
RR-lt
RR-2f
Subtotal - Re-refining
Total
Number
of
Facilities
50
65
60
20
20
25_
240
3
12
13
253
Model
Facility
Annual
Volume
(1Q3 gal)
750
1,500
2.500
2.500
2.500
7,500
3.500
8,000
.
Total
Annual
Volume
(106 gal)
37.5
97.5
150.0
50.0
50.0
187.5
572.5
10.5
80.0
90.5
663.0*
Percent
of
Total
Processed
Oil
6.6
17.0
26.2
8.7
8.7
32.8
100.0
-
-
Estimated
Oil . ,
Handled by
Each Mode It
34.3
88.4
136.3 (139.4)**
45.3 (46.3)**
45.3 (46.3)**
170.6 _(1?4.7)**
520.2 (529.4)**
10
21
85
605.2 (614.4)**
This value is greater than the total estimated volume of material handled by processors and
re-refiners (605.2 mil gal). Some disagreement is expected because the total annual volume
was calculated based upon typical facility volumes rather than average volumes. Since the
actual number of facilities was factored with typical volumes, agreement in total volume
would be mere coincidence.
t The number of re-refining facilities and volumes of oil handled were independently estimated
and held fairly constant in this analysis because a high level of confidence exists in those
estimates.
J The estimated volumes passing through the processor models were calculated to fit the oil volume
which remained following the subtraction of the re-refiner estimates. For example, the oil flow
through MP-1 was calculated by:
(520.2) x 0.066" 34.3 million gallons.
** The volumes shown in parentheses for major processors and re-refiners are adjustments associated
with oil received from minor processors. In effect, this is double counting. Although only
605.2 million gallons enter the system, 614.4 million gallons are actually handled because of
inter-facility transfers. See code (1) for a description of minor processor oil distribution
practices.
C-13
032G
-------
Adjustments in the volume of oil handled by each major
processor type (Kls) is shown in Table C-4 in parentheses.
These adjustments represent oil which passes from minor
processors to major processors as part of normal flows
(see letter codes "1" and "m"). Therefore, the actual
volume of oil handled is somewhat higher than the amount
entering the UOMS.
(1) The distribution of product oil from the selected pro-
cessing and re-refining model facilities is based upon
the results of a limited survey of companies. Table C-5
summarizes the percent distribution of product oil from
processors, re-refiners, and independent collectors.
These estimates were taken directly from the detailed
market analyses developed for each model facility.
Also, included in Table C-5 is the calculated distribu-
tion of all input oil including product oil and oil losses
and disposal in processing residues. Since residue gen-
eration and disposal practices vary tremendously for
different facility types, it was estimated that a 5 per- .
cent loss factor is common for processing facilities.
The disposal estimates shown for re-refiners is greater and
based upon reported practices as obtained in the company
survey. The output gallonage for each model was calcu-
lated from the percentages shown in Table C-5 and the
estimated input to the facilities (k).
(m) The amount of used oil handled "twice" by the UOMS (once
by minor processors and once by major processors or re-
refiners) was calculated from the outputs from the two
minor processors models classified as the "major proces-
sor/re-refiner" market.
(MP-1) - 4.8 mil gal
+(MP-2) - 4.4 mil gal
Total 9.2 mil gal
(n) Total re-refined lube oil is equal to the sum of lube oil
produced by the acid-clay and vacuum distillation re-re-
finer models.
(o) Non-fuel industrial uses for product oil includes flo-
tation oil for the phosphate industry, and material
feedstock for asphalt manufacture, and form oil. The
total oil consumed for this purpose is the non-fuel
industrial output from the processor models and the
bottoms material produced by vacuum distillation
re-refiners.
C-14
FRANKLIN ASSOCIATE
-------
Table C-5
SUMMARY OF USED OIL DISTRIBUTION FROM MODEL FACILITIES*
(percent)
Virgin Other
Direct Oil Processors
Fuel Fuel Non-Fuel Road or
Model Facility Sales Dealer Industrial Oiling Re-refiners
Collector Only 9.5Z 9.5Z - 147 62Z
Minor Processors
MP-1
Product Oil 25 45 5 10 15
Total Oil Input 24 43 5 9 14
MP-2
Product Oil 30 50 5 5 5
Total Oil Input 28 47 5 5 5
Major Processors
MJP-1 and MJP-2
Product Oil 45 40 8 2 -
Total Oil Input 43 38 7 2 -
MJP-3 and MJP-4
Product Oil 60 30 3 2 -
Total Oil Input 57 28 3 2 -
Re-Refiners
RR-1 _____
RR-2 - 12 -
On-Site
Fuel
-
-
5
5
5
5
5
5
n
n
Lube Oil Disposal Total}
65
75
5Z
28
6
100
100
100
100
100
100
100
100
100
100
100
* Used oil distribution is described as the percent of total oil output. For the processor models, two sets
of percentages are shown. The first shows product oil distribution only; the second is based upon total
oil input and includes oil losses in disposal residues.
t Sum of calculated percents as related to total oil input may not equal 100 due to rounding.
J It was assumed that the recovered distillate fuels are burned in-house for process heating.
Source: Franklin Associates. Ltd., from a limited survey of facilities including site visits (C-15).
C-15
0327
-------
(p) Total used oil sales through virgin oil fuel dealers
was calculated as the flume of V.O.F.D. outputs from
the processor and Independent collector models.
(q) Total burned used oil equals the sum of (1) burning
by DIYers, (2) fuel use by generators, (3) fuel sales
by all processors and collectors, (4) V.O.F.D. sales,
(5) distillate fuel production by re-refiners, and
(6) on-site burning by processors.
(r) The estimate of the volume of used oil burned In large
and small boilers was calculated as the difference in
the total oil burned and the sum of oil burned in cement
kilns, diesel engines, space heaters, and on-site boilers.
(s) Cement companies routinely burn waste materials along
with conventional fuels to provide the large .amounts
of heat required for cement kiln operation. The pub-
lished fuel statistics for this industry do not dis-
tinguish between u iste fuels consumed which include
used oils, solvents, and contaminated fuel oils (C-6).
The Portland Cement Association reports that used oil use
is not significant, but some may .be used with consumption
ranging from 0 to 10 million gallons per year (C-7). For
this study, the midpoint volume of 5 million gallons per
year was ae°imifi'^r
(t) and (u) Used oil burned in diesel engines and space
heaters was previously evaluated in the letter (d)
discussion which examined generator used oil use as
a fuel.
(v) Processors and re-refiners burn used oil and light dis-
tillates recovered through processing to provide on-site
process heat and sometimes space heat for buildings. From
the processor survey, it was estimated that approximately
3 percent of product oil is burned on-site. Re-refiners
often burn the recovered distillate fuels which comprise
about 7 percent of input used oil (C-ll). In total,
on-site burning by processors and re-refiners was esti-
mated to be 30.7 million gallons in 1983.
Also included in the on-site boiler use -is burning by
industrial facilities (see letter "f" - 37.1 million
gallons) and the burning of primarily automotive oils
by military bases (see letter "d2" - 6.1 minion gallons).
Overall, a total of 73.9 m-tlljon gallons were believed to
be burned in on-site boilers In 1983.
C-16
PRANKUN ASSOCIATES
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(w) Total road oiling was estimated by summing the road
oiling activity of each processor model, the inde-
pendent collector model, and in-house generator usage.
(x) and (y) Used oil disposal primarily includes the con-
ventional techniques of landfilling and incineration
and the undesirable method of dumping. Some oil may
enter into disposal lagoons or the municipal sewer.
systems, but overall, these avenues of disposal are
believed to be of minor significance. For this analysis,
it is not possible to totally distinguish between land-
filling and incineration methods; however, industrial
oils are about 5 times more likely to be land disposed
than incinerated (see Table C-3).
Some oil is disposed of at every stage in the UOMS.
The DIYer may put the oil in the municipal solid waste
stream; the industrial generator may have a private
hauler dispose of a highly contaminated used oil; and
processors and re-refiners produce sludges with variable
oil contents for disposal. The (x) value is the sum of
these disposal estimates for each selected UOMS model,
as well as the generators.
Used oil which is dumped (letter "y") originates from two
basic sources: (1) DIYers and (2) off-road vehicle oper-
ators. According to the DOE DIYer study (C-l), about 60
percent of the oil generated by DIYers is dumped. The
dumping of oil generated by off-road vehicles has been
previously discussed in the generator use disposal
section (d4).
C-17
0328
FRANKLIN ASSOCIATES, LTD.
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APPENDIX C REFERENCES
C-l Gottlieb, J., "Analysis of Potential Used Oil Recovery from Individ-
uals," DOE/BC/10053-21, 1981.
C-2 Weinstein, N. J., "Waste Oil Recycling and Disposal," Recon Systems,
Inc., for the U.S. Environmental Protection Agency, August 1974.
C-3 Resource Technology, Inc., RTI Newsletter, 1982.
C-4 Development Planning and Research Associates, Inc., "Selected Charac
teristics of the Waste Oil Space Heater Industry." EPA Contract No.
68-02-3173, July 1983.
C-5 Development Planning and Research Associates, Inc., "Interim Report
for the RCRA Economic Impact Analysis of the Effects of the Waste
Oil Regulations on the Waste Oil Management SystemSystem Descrip-
tion." EPA Contract No. 68-01-6322, May 1981.
C-6 Portland Cement Association, Energy Report, U.S. Portland Cement
Industry, August 1982.
C-7 Personal communications with Rob Roy, Portland Cement Association,
October 20, 1982.
C-8 Richard J. Bigda & Associates, "Review of All Lubricants Used in
the U.S. and Their Re-refining Potential," prepared for the Bartles
vill Energy Technology Center, U.S. DOE, June 1980.
C-9 U.S. Department of.Commerce, Bureau of Census, Census of Manufactui
1977 and 1982.
C-10 U.S. Department of Commerce, Bureau of Industrial Economics, 1984
U.S. Industrial Outlook.
C-ll U.S. EPA, "EPA Survey of Handlers and Burners of Used or Waste Oil
and Waste-Derived Fuel Material," survey performed 1983-1984, data
obtained from computer files.
C-12 Brecht, F., "Outlook for U.S. Lube Oil Supply and Demand," present
at the 1983 National Petroleum Refiners Association Annual Meeting
by Pennzoil Products Company, March 20-22, 1983, San Francisco.
C-13 1981 Commercial Car Journal Fleet Census.
C-18
FRANKLIN ASSOCIATE
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C-14 Fu, T. T., and C. Semien, "Utilization of Navy-Generated Waste Oils
as Boiler Fuel - Handbook of Guidelines and Field Survey Results,"
Naval Civil Engineering Lab, Port Hueneme, California, August 1983.
C-15 Franklin Associates, Ltd., survey of selected industries and site
visits to industrial establishments to assess used oil generation
and management practices, information obtained May 1983 to August
1984.
C-19
0329
FRANKLIN ASSOCIATES, LTD.
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Appendix D
ALTERNATIVE METHOD TO CALCULATE MEAN CONCENTRATION
OF HAZARDOUS CONSTITUENTS IN USED OIL
There was some question among the research team and the U.S. EPA
regarding the most appropriate method to calculate the mean concentration
of hazardous constituents. Throughout this report mean concentrations
are presented for detected concentrations only. Non-detected values vere
not included in those calculations because detection limits varied signif-
icantly. For example, many PCS tests had a detection limit of 50 ppm, but
others could measure concentrations down to 1.0 ppm. It seemed inappropriate
to consider samples with levels of <50 ppm and <1 ppm equal to zero, or even
equal to their detection limits. There seemed to be no single method which
would avoid distortion. That is why means were calculated for detected
values only throughout this report.
Nevertheless, some individuals believed that the conservative
approach of assuming the concentration to be equal to the detection limit
to be the most appropriate for some risk assessment calculations. For this
reason, an alternative mean was calculated for each contaminant for most
used oil types. Table D-l shows these values assuming that the concentration
of the contaminant in a non-detected situation was equal to the detection
limit (e.g., <50 « 50; <1 - 1).
D-l
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