530SW013
PB88-111752
NOT&
Information is our business.
COMPOSITION AND MANAGEMENT OF USED OIL
GENERATED IN THE UNITED STATES
FRANKLIN ASSOCIATES, LTD.
PRAIRIE VILLAGE, KS
SEP 84
EP 530
SW-013
App.
MENT OF COMMERCE
inical Information Service
-------
APPENDIX
COMPOSITION AND MANAGEMENT OF USED OIL
GENERATED IN THE UNITED STATES
Prepared for
U.S. ENVIRONMENTAL PROTECTION AGENCY
By
FRANKLIN ASSOCIATES, LTD.
8340 Mission Road
Suite 101
Prairie Village, Kansas 66206
Septe-ber 1984
REPRODUCED BY
U.S. DEPARTMENT OF COMMERCE
NATIONAL TECHNICAL INFORMATION SERVICE
SPRINGRELD. VA. 22161
-------
0272 -101 ^ .
REPORT DOCUMENTATION
PAGE
. REPORT NO.
N/A
I. Title ind Subtitle
Appendix - Ccmp^sitio"! and Management of Used
Oil Generated iv the United States
3. Recipient's Accession No.
B^W-W
5. RepoTTo.** * -• fc O *
September 1984
7. Author(s)
8. Performing Organization Rept. No.
Franklin Associates, Ltd.
9. Performing Organisation Name and Address
Franklin Associates, Ltd.
8340 Mission Road
Suite 101
Prairie Village, Kansas 66206
10. Project/Task/Work Unit No.
11. Contract(C) or Grant(G) No.
(C) N/A
(G)
12. Sponsoring Organization Name and Address
U.S. Environmental Protection Agency
Office of Solid Waste
401 M Street, S.W.
Washington, D.C. 20460
13. Type of Report & Period Covered
Final
14.
15. Supplementary Notes
This appendix supplements "Composition and Management of Used Oil Generated in
the United States" (November 1985) - NTIS Accession Number PB85-180 297.
16. Abstract (Limit: 200 words)
This document is an appendix to the report entitled "Composition and Management
of Used Oil Generated in'the United States" which characterizes used oil generation,
management, and composition in the United' States in 1983. The study was carried out
to provide the U.S. Environmental Protection Agency with the needed background
information to develop the most appropriate used oil regulations and to provide a
framework for assessing the risks and benefits of alternative regulatory options.
This document contains four appendices: A = Analytical Data for Waste Oil
Samples; B = Data Base for Contamination of Residues from Waste Oil Processing
and Re-refining; C = Methodology and References for Used Oil Flow Description; D =
Alternative Methodology to Calculate Mean Concentration of Hazardous Constituents
in Used Oil.
17. Document Analysis a. Descriptors
b. Identifiers/Open-Ended Terms
C. COSATI Field/Group
18. Availability Statement
Release Unlimited
19. Security Class (This Report)
Unclassified
20. Security Class (This Page)
Unclassified
21. No. of Pages
22. Price
-------
-------
-------
-------
NOTICE
THIS DOCUMENT HAS BEEN REPRODUCED FROM
THE BEST COPY FURNISHED US BY THE SPONSORING
AGENCY. ALTHOUGH IT IS RECOGNIZED THAT CER-
TAIN PORTIONS ARE ILLEGIBLE, IT IS BEING RE-
LEASED IN THE INTEREST OF MAKING AVAILABLE
AS MUCH INFORMATION AS POSSIBLE.
-------
TABLE OF CONTENTS
Appendix Title Page
A ANALYTICAL DATA FOR WASTE OIL SAMPLES A-l
B DATA BASE FOR CONTAMINATION OF RESIDUES FROM B-l
WASTE OIL PROCESSING AND RE-REFINING
C METHODOLOGY AND REFERENCES FOR USED OIL FLOW C-l
DESCRIPTION
D ALTERNATIVE METHODOLOGY TO CALCULATE MEAN D-l
CONCENTRATION OF HAZARDOUS CONSTITUENTS IN
USED OIL
0233
-------
-------
APPENDIX A
ANALYTICAL DATA FOR WASTE OIL SAMPLES
Appendix A presents a comprehensive analytical data base for more
than 1,000 waste oil samples. Table A-l provides the raw data for all samp-
les numbered consecutively from 1 to 1,071. Over 200 of these sample results
were developed as part of EPA's 1983 used oil sampling program. For these
samples, EPA sample numbers are shown in parentheses beside the consecutive
numbering selected for this study. Table A-2 provides the sources from which
oil analytical data were received, and Table A-3 provides letter codes for
each sample number which describe the specific used oil generating source and
end-use for the oil, if known.
A-l
0234
-------
TABLE A-I
ANALYTICAL DATA FOR USED OIL SAMPLES
Sample Number*
Flash Point (T)
Metals
Arsenic
Aluminum
Barium
Beryllium
Cadmium
Chromium
Cobalt
Copper
Iron
Lead 1
Magnesium
Manganese
Molybdenum
Nickel
Selenium
Silicon
Silver
Sodium
Tin
Titanium
Vanadium
Zir.c 1
Volatile Organics
Dichlorodif luoroDCthane
TrichlorofluoTOMthane
I
174
13
16
22
0.06
1.9
6.3
<0.04
36
290
.590
380
19
6.8
1.3
<0.3
19
<0.01
140
11
0.3
<0.1
.150
<20
<20
Tr ichlor otr if luoroethane< 20
1.1,1-Trichloroethan*
Trichloroethylene
Te trachloroe thy lene
Phencl
Benzene
Toluene 1
Ethvl Benzene
Xylenes 2
Me thy lene Chloride
FNAs
Naphthalene
Phenanthrene /Anthracene
Pyrene
Benzo(a)anthracene
Benzo(a)pyrene
Alkvlbenzene (C9H12) 2
Alkylnaphthalene (C12H12)
Phosphorus
Chlorine, wt. *
Sulfur, vt. I
PCBs
100
<20
700
<20
100
,650
800
,300
<20
560
150
110
d.0
^10
.700
-
-
0.16
1.02
160
3.7
15
49
<0.04
<0.8
3.3
0.2
27
100
510
260
3.1
1.4
0.7
<1.0
34
<0.04
150
1.1
1.1
<0.2
660
<20
<20
530
210
220
<20
<10
80
2,800
730
2,400
<20
170
130
10
^10
^10
<20
-
-
0.10
0.72
168
14
13
160
0.04
2.3
5.2
<0.1
39
180
1.630
380
11
8.7
1.1
<0.8
21
0.2
93
8.4
0.3
<0.2
1,020
<20
<20
<20
950
<20
900
<10
<20
1,400
580
220
<20
260
40
10
<10
<10
33,000
-
-
0.19
1.29
4
200
11
17
62
0.04
1.0
3.8
<0.06
73
140
1.280
310
12
2.9
1.4
<0.5
20
0.3
110
21
0.4
<0.1
920
<20
<20
<20
120
<20
<20
<10
180
1.200
320
-
<20
240
80
20
20
<10
-
-
-
0.10
0.75.
13
5_
17
8.3
150
0.04
0.8
3.4
0.2
13
110
2.060
280
13
1.4
0.6
<0.4
22
<0.4
60
2.2
2.2
<0.2
630
<20
<20
<20
<20
<20
<20
<40
90
670
160
710
<20
280
130
20
10
<10
<20
-
-
0.12
0.87
jb
200
<0.4
8.4
9.2
<0.01
0.6
0.3
<0.04
91
58
23
590
1.4
3.5
0.3
<0.3
8.2
<0.01
24
16
<0.01
<0.1
1,550
<20
<20
<20
<20
<20
<20
<10
100
1.700
260
880
<20
490
140
40
40
<10
6,600
-
-
0.05
0.94
192
17
11
95
0.03
1.6
4.1
<0.1
23
170
1.890
320
14
4.5
1.2
<0.7
14
0.03
100
8.6
0.2
0.2
1,000
<20
<20
<20
130
130
<20
<10
70
2,300
840
-
<20
580
210
40
20
<10
-
-
-
0.12
0.78
:
-
22
460
-
-
21
-
17
260
7 "XX)
1 XX)
3
10
0
-
18
0
51
c
-
0
1, 00
-
-
-
-
-
••
-
-
-
-
-
-
-
-
1.400
-
-
2
-
10
36
-
-
3
-
18
180
75
1.100
0
4
0
-
-
0
39
3
-
0
1.300
-
-
-
-
-
-
-
-
-
-
-
-
-
-
-
-
-
-
-
1,400
-
-
* Table A-2 identifies the source of analytical data for each used oil sample. Table A-3 provides
codes for each sample number which describe the specific generating source of used oil and the end-use.
A-2
-------
TABLE A-l (continued)
ANALYTICAL DATA FOR USED OIL SAMPLES
Sample Number*
Flash Point (*F)
Metals
Arsenic
Aluminum
Bariua
BervIlium
Cadmium
Cr.romium
Cobalt
Copper
Iron
Lead
Magnesium
Manganese
Molybdenum
Nickel
Selenium
Silicon
Silver
Sodium
Tin
Titanium
Vanadium
Zinc
Volatile Organics
Dichlorodifluoromethane
Trichlorofluoronethane
Trichlorotrifluoroethane
1,1,1-Trichloroethane
Tetrachloroethylene
Pheno!
. Benzene
Toluene
Ethyl Benzene
Xylenes
Methylene Chloride
10
398
U.
360
13
430
9
451
0
43
115
0
990
ii
370
14
485
380
13
428
380
10
260
380
12
203
255
7
144
0
25
72
0
668
0
39
95
0
780
0
38
660
0
860
0
36
102
0
1,233
0
27
89
0
910
IT.
350
21
278
24
16
292
7,039
-
-
22
119
6.495
225
3
43
203
7,595
165
4
41
150
6,560
259
2
41
129
4,890
227
8
38
212
10,410
458
3
37
116
4,165
261
2
37
655
8.005
297
8
0
87
357
0
1,040
Naphthalene
Phenanthrene/Anthracene
Pyrene
Benzo(a)anthracene
Ber,zo(a)pyrene
Alkylbenzene (£7^12^
Alkylnaphthalene (C^H^)
Phosphorus
Chlorine, wt X
Sulfur, wt X
PCBs
871
0.50
672
0.40
815
0.46
764
0.46
1,015
0.53
708
0.45
778
0.33
* Table A-2 identifies the source of analytical data for each used oil sample. Table A-3 provides
codes for each sample number which describe the specific generating source of used oil and the end-use.
A-3
0235
-------
TABLE A-l (continued)
ANALYTICAL DATA FOR USED OIL SAMPLES
Plash Point CD
Metals
Arsenic
Aluminum
Barium
Beryllium
Cadmium
Chromium
Cobalt
Copper
Iron
Lead
Ma»r.2sium
Manganese
Molybdenum
Nickel
Selenium
Silicon
Silver
Sodium
Tin
Titanium
Vanadium
Zinc
18
375
-
11
'520
-
-
8
-
18
179
4,560
182
4
-
2
-
37
-
100
-
-
0
660
19_
250
-
13
333
-
—
8
-
41
173
7.680
209
3
-
2
-
32
-
61
-
-
0
1.140
Sample
22 21
355 215
-
20
319 568
-
— -
11
-
31
216 356
7,570 11.100
375
4
-
2
-
51
-
125 .
-
-
0 <5
980 800
Number*
22_
204
-
12
180
-
-
9
-
33
137
4,720
311
3
—
1
-
<15
-
64
6
-
0
1,201
23
427
-
27
693
-
~
22
-
33
306
13,885
325
4
-
1
-
<15
-
42
7
-
0
1,267
2i
360
-
15
286
-
-
12
-
27
200
7.070
236
3
-
1
-
<15
•
142
2
-
0
1,000
11
403
-
12
„ 175
-
-
14
-
27
162
5,223
323
8
-
1
-
<15
-
41
2
-
0
952
26_
144
-
_
.
-
-
.
-
-
.
90
-
-
-
-
-
-
-
-
-
-
-
-
Volatile Organics
Dichlorodifluoromethane
Trichlorofluoromethane
Trichlorotrifluoroethane
1,1.1-Trichloroethane
Tncr.ioroethyiene
Tetrachloroethvlene
Phenol
Benzene
Toluene
Ethyl Benzene
Xylenes
Methylene Chloride
P.NAs
Naphthalene
Thenanthrene/Anthracene
Pvrene
Benzo(a)anthracene
Benzo(a)pyrene
Alkylbenzene (C7H12)
Alkylnaphtnalen* CC.-H -)
Phosphorus
Chlorine, vt Z
Sulfur, wt X
PCBs
674
0.41
996
0.44
961
0.41
900
0.34
1.080
0.39
1,118
0.38
889
0.36
1,060
0.45
0.
* Table A-2 identifies the source of analytical data for each used oil sample. Table A-3 provides
codes for each sample nunber which describe the specific generating source of used oil and the end-use.
A-4
-------
TABLE A-l (continued)
ANALYTICAL DATA FOR USED OIL SAMPLES
Flash Point CD
Metal
Arsenic
Aluminum
Bariuo
Beryllium
C«c=iuz
Chromium
Cobalt
Copper
Iron
Lead
Magnesium
Manganese
Molybdenum
Nickel
Selenium
Silicon
Silver
Sodiua
Tin
Titanium
Vanadium
Zinc
Volatile Organics
Dichlorodifluoromethane
Trichlorofluoromethane
Trichlorotrifluoroethane
- .1,!-Trichloroethane
7rur.icroech> lene
Tetrachloroethylene
Phenol
Benzene
Toluene
Ethyl Benzene
Xylenes
Methylene Chloride
PNAs
Naphthalene
Phenanthrene/Anthracene
Pyrene
Ben2oi,a)anthracene
8enzo(a)pyrene
Alkylbenzene (CgH,,)
Alkylnaphthalene tc.,H..)
Phospt-ctus '
Chlorire, wt Z
Sulfur, wt Z
PCBs
II
367
131
740
0.44
398
13
148
10
1,012
0.38
li
222
10
229
10
12
365
15
176
12
Sample Number*
406
15
204
12
32_
335
12
124
21
782
0.42
1,138
0.45
1,074
0.34
895
0.54
23
440
17
185
35
1
"<15
55
5
0
629
1
"«15
132
6
0
1.239
2
"<15
207
3
0
1.023
1
19
54
4
0
1.316
1
"«13
79
3
0
1,151
1
"<15
8
3
0
1,169
4
25
!*5
0
2.500
1.393
0.44
315
11
•94
12
17
164
3.730
138
8
26
222
8,460
384
6
39
151
5.860
236
3
20
249
10,560
425
3
31
212
8,450
312
3
6
170
11,575
599
2
7
133
7.730
999
2
37
181
7.825
286
3
5
" 40
127
0
933
23
440
76Q
747
0.40
<5
* Table A-2 identifies Che source of analytical data for each used oil sample. Table A-3 provides
codes for each sample number which describe the specific generating source of used oil and the end-use.
A-5
023G
-------
TABLE A-l (continued)
ANALYTICAL DATA FOR USED OIL SAMPLES
Sample Number*
Flash Point ("F)
Metals
Arsenic
Aluminum
Barium
Beryllium
Cadmium
Chromium
Cobalt
Copper
Iron
Lead
Magnesium
Manganese
Molybdenum
Nickel
Selenium
Silicon
Silver
Sodium
Tin
Titanium
Vanadium
Zinc
36
405
_
14
200
-
-
11
-
13
178
6,885
171
2
—
4
-
8
-
150
-
-
0
705
2£
380
_
19
494
-
»
6
-
56
171
6,980
220
3
—
<1
-
16
-
23
6
-
0
1,409
38_
310
•
4
10
-
-
8
-
13
88
19
8
1
-
<1
-
14
-
67
•0
-
0
80
39
405
^
13
297
-
-
10
-
28
192
4,855
520
3
—
<1
-
26
-
59
i,
-
0
1.029
40
355
^
6
377
-
-
5
-
12
102
1.362
147
2
—
<1
-
15
-
34
3
-
0
1.527
4_1
305
_
18
547
-
-
12
-
27
216
8.655
233
4
—
1
-
25
-
64
1
-
0
725
42.
370
18
213
-
—
10
-
37
272
9,420
310
4
—
2
-
17
-
169
8
-
0
1.150
43
365
" 25
59
-
•
14
-
16
342
11,165
338
4
—
1
-
14
-
69
14
-
0
1.574
ii
_
_
-
-
-
-
-
-
-
-
-
-
-
-
-
-
-
-
-
-
-
-
-
Volatile Organic:
Dichlorodiflucronethane
Trichlorofluoromethane
1r_c~-:r-i: _;'luorce thane
1,1,1-Trichloroethane
Trichloroethylene
- Tetrachloroethylene
Phenol
Benzene
Toluene
Ethyl Benzene
Xylenes
Mechylene Chloride
PHAs
Naphthalene
Phenanthrene/Anthracene
Pyrene
Benzo(a)anthracene
Benzo(a)pyrene
Alkylbenzene (CgH^)
Alkylnaphthalene (C1,En.)
Phos
Chlo
Sulf
PCBs
3.2-16
iphorus
irine, wt Z
:ur, wt %
" 675 982 81 880 1,197 857 881 1,341
0.22 0.40 0.37 0.35 0.46 0.38 0.38 0.47
* Table A-2 identifies the source of analytical data for each used oil sample. Table A-3 provides
codes for each sample number which describe the specific generating source of used oil and the end-use.
A-6
-------
TABLE A-l (continued)
ANALYTICAL DATA FOR USED OIL SAMPLES
Sample Number *
Flash Point (*F)
Metala
Arsenic
Aluminum
Barium
Beryllium
Cadmium
Chromium
Cobalt
Copper
Iron
Lead
Magnesium
Manganese
Holybdenum
Nickel
Selenium
Silicon
Silver
Sodium
Tin
Titanium
Vanadium
Zinc
Volatile Organics
Dichlorodifluoroaethane
Trichlorofluoromethane
Irichlorotrifluoroeehane
1.1,l-7r;.;hloroeshane
Tricnioroethvlene
Tetrachloroethylene
Phenol
Benzene
Toluene
Ethyl Benzene
Xylenes
Methylene Chloride
PSAs
Naphthalene
Phenanthrene/Anthracene
Pyrene
Benzo(a)anthracene
Benzo(a)pyrene
Alkylbenzene (CgKp)
Alkylnaphthalene (C.-H.,)
Phosphorus
Chlorine, wt Z
Sulfur, wt Z
PCBs
45
295
46
47
4jB 49_
50
-
-
-
-
-
_
1.025
6,000
559
-
-
-
_
-
158
-
-
21
-
.
2-1,631
-
-
-
1-120
10-330
1-11.000
3-500
1-200
-
-
-
-
-
-
-
-
560-1,550
14
150
-
-
10
4
149
10,420
47
2
-
2
12
-
18
10
-
0
461
10-800
10-2 .000
6
4
8-50
5-348
50-2,000
800-21.700
10-1.108
5-10
2-3
3-30
10-875
1
16-300
5-112
5-30
3-39
300-3,000
33
200
-
2
27
50
750
7,800
430
42
7
3
47
0
160
20
5
5
1,100
600-1,410
0.03-0.49
0.43 0.13-0.47
600 500-2,000
0.21-0.65
900
6.000
1.000
1,000
* Table A-2 identifies the source of analytical data for each used oil Maple. Table A-3 provides
codes for each sample number which describe the specific generating source of used oil and the end-use.
A-7
0237
-------
TABLE A-l (continued)
AKALYTICAL DATA FOR USED OIL SAMPLES
Sample Number*
51
175-427
52
£5
350
54
205
55
li
32.
365
15
Flash Point CF)
Metals
Arsenic
Aluminum
-------
TABLE A-l (continued)
ANALYTICAL DATA FOR USED OIL SAMPLES
Sample Number*
12 60
Flash Point (°F) - 300
Metals
Arsenic
Aluminum
Barium 200 <100
Beryllium
Cadcius - .
Chromuxo — .
Cobalt
Copper 20 45
Iron 180 105
Lead 3,300 1.100
Magnesium
Manganese
Molybdenum
Nickel
Selenium
Silicon
Silver
Sodium
Tin
Titanium - -
Vanadium -
Zinc 460 680
Volatile Organics
Dichlorodif luoromethane
Trichlorof luoromethane
Trichlorocrifluoroethane
1 . 1 , 1-Trichloroethane
Incruoroe^nvlene
Tetrachloroethylene
Phenol
Benzene
Toluene
Ethyl Benzene
Xylenes
Methylene Chloride
PSAs
Naphthalene
Phenanthrene /Anthracene
Pyrene
Benzo (a) anthracene
li i£ ii *i
105
13.95
- - - 10.2
310 <100 <100 59.5
- 0.05
- 2.1
7.1
0.16
45 65 25 45.7
300 515 210 163
2,450 2,210 3,300 1,417
200
7.5
3.8
2.0
0
0
o
132
9.1
1.3
2.1
680 480 680 743
- ...
50
....
1,600
38
185
- 5.100
- 1.150
....
- ...
- 440
90
38
- 16
.65 66 6]_
221 220 215
13 16
' - 600
. -
3 4 -
3 3 -
34 36 360
159 177 11,100
-
- .
- -
...
- .
10 12
...
<5 <5
- .
800
...
. — .
...
— - —
.
- - -
. -
» - -
...
. - _
...
- .
•» - _
— — _
» -
- - -
Benzo(a)pyrene
Alkylbenzene (C7H.,)
Alkylnaphthalene tc.-Hj.)
Phosphorus
Chlorine, wt t
Sulfur, wt X
PCBs
1.230
0.34
0.52
980
0.05
0.43
1,380
0.06
0.60
1,500
0.44
0.49
1.330
0.14
0.59
0.20
0.48
900
0.34
* Table A-2 Identifies the aourc* of analytical data for each uaed oil (ample. Table A-3 provides
codes for each sample number which describe the specific generating source of used oil and the end-use.
A-9
0238
-------
TABLE A-l (continued)
ANALYTICAL DATA FOR USED OIL SAMPLES
Sample Number*
68 M
Flash Point CF) 375 175
Metals
Arsenic <5 <5
Aluminum
Barium 1.000 100
Beryllium
Cadmium
Chromium
Cobalt
Copper
Iron - 200 90
Lead 9.000 7,200
Magnesium - -
Manganese
Molybdenum
Nickel
Selenium
Silicon
Silver
Sodium
Tin
Titanium
Vanadium - -
Zinc 700 350
Volatile Organics
Dichlorodifluoronethane
Trichlorofluoronethane
Trichlorotrlfluoroethane
1 , 1 , 1-Trichloroethar.e
Trichloroethylene
Tetrachloroethylene
Phenol
Benzene
Toluene
Ethyl Benzene
Xylenes -
Methylene Chloride
PSAs
Naphthalene
Phenanthrene/ Anthracene -
Pyrene
Benzo(a)anthracene
Benzo(a)pyrene
Alkylbenzene
Alkyln«phth«lene (C.-H )
Phosphorus * 1.000 550
Chlorine, wt Z -
Sulfur, ut Z - 0.29
PCBs
* Table A-2 identifies the source of analytical data for each used oil sample. Table A-3 provides
codes for each sample number which describe the specific generating source of used oil and the end-use.
A-10
-------
TABLE A-l (continued)
ANALYTICAL DATA FOR USED OIL SAMPLES
Flash Point (°F)
Metals
Aluminum
Arsenic
Barium
Beryllium
Cadmium
Chromium
Cobalt
Copper
Iron
Lead
Magnesium
Manganese
Molybdenum
Nickel
Selenium
Silicon
Silver
Sodiirr.
Tin
Titanium
Vanadium
Zinc
Volatile Organics
Dichlorodifluoromethane
Tnchl rrr:luoroaethar.e
Tricniorotrifluoroethane
1,1,1-Trichloroethane
Trichlorcethylene
Tetrachloroethylene
Phenol
Benzene
Toluene
Ethyl Benzene
Xylenes
Methylene Chloride
PNAs
Naphthalene
Pher.anchrene/Anthracene
Pyrene
Benzo(a)anthracene
Benzo(a)pyrene
Alkylbeazene (C.H )
Alkylnaphthalene ^ " s
Phosphorus
Chlorine, wt. %
Sulfur, wt. %
PCBs
n!2
Sample Number*t
22 (262) 21(263) 11 (264) 21
158 164 164
16
<5
29
<0.2
1.6
5.8
<0.5
33
200
1,300
420
11
1.6
110
74
75
76
77
860
220
2,000
500
1,700
1,000
0.07
0.59
<5
15
<5
14
<0.2
1.5
6.2
<0.5
29
220
300
400
13
15
<5
11
<0.2
2.1
6.0
<0.5
34
230
1,400
470
13
1.7
160
160
<0.2 <0.2 <0.2
1,100 1,100 1,100
3,000
<39
<39
140
760
360
1,400
<39
0.05
0.61
<5
1,000
0.85
0.54
<5
10
11
10
11
* Table A-2 identifies the source of analytical data for each used oil sample. Table A-3 provides
codes for each sample number which describe the specific generating source of used oil and the end-use.
t Numbers in parentheses represent EPA sample numbers for used oil samples obtained as part of their
1983 sampling program.
A-ll
0233
-------
TABLE A-l (continued)
ANALYTICAL DATA FOR USED OIL SAHPLES
Sample Number*
Flash Point (°F)
Metals
Aluminum ________
Arsenic ________
Barium - - - - - - _ ., _
Beryllium - - - - - _ • _
Cadmium ________
Chromium ________
Cobalt ________
Copper ________
Iron ________
Lead ________
Magnesium ________
Manganese ________
Molybdenum ________
Nickel ________
Selenium ________
Silicon ________
Silver ________
Sodiura ________
Tin ________
Titanium ________
Vanadium ________
Zinc ________
Volatile Organics '
Dichlorodifluoromethane ________
Trichlorofluoromethane ________
Trichlorotrifiuoroethane __-__-__
1,1,1-Trichloroethane ________
Trichloroethylene ________
Tetrachloroethylene ________
Phenol ________
Benzene ________
Toluene ________
Ethyl Benzene • - - ___-
Xylenes - - - - -'-
Methylene Chloride - - - - - - - - -
PNAs
Naphthalene _______*.
Phenanthrene/Anthracene ________
Pyrene ________
Benzo(a)anthracene ______ _-
Benzo(a)pyrene 14 14 . 16 12 14 17 1.5 1.3
Alkylbenzene
AlkylnaphthalenI
Phosphorus
Chlorine, wt. %
Sulfur, wt. %
PCBs
* Table A-2 identifies the source of analytical data for each used oil sample. Table A-3 provides
codes for each sample number which describe the specific generating source of used oil and the end-use.
A-l 2
-------
TABLE A-l (continued)
ANALYTICAL DATA FOR USED OIL SAMPLES
Sample Number*
M JLl M li .22 ii 11
Flash Point (°F)
Metals
Aluminum _______
Arsenic ____--_
Barium _______
Beryllium _______
Cadmium _______
Chromium _______
Cobalt _______
Copper __.-_-__
Iron ___--__
Lead _______
Magnesium _______
Manganese __-__-_
Molybdenum _______
Nickel _______
Seieniua _______
Silicon _-_---_
Silver _______
Sodium _______
Tin _,__---
Titanium _______
Vanadium _.__---_
Zinc ____---
Volatile Organics
Dichlorodifluoromethane _______
Trichlorofluoromethane _______
Tricr.-croirifluoroethane ____---
1,1,1-Trichloroethane _______
Trichloroethylene ____---
Tetrachloroethylene _______
Phenol __-----
Benzene ___----
Toluene _______
Ethyl Benzene _______
Xyler.es _______
Methylene Chloride ___----
PNAs
Naphthalene _______
Phenanthrene/Anthracene ____---
Pyrene ___----
Benzo(a)anthracene ____-_-
Benzo(a)pyrene 1.7 1.3 12 3.2 16 14 5.2
Alkylbenzene (CgH.,)
Alkylnaphthalene tC12
Phosphorus
Chlorine, wt. %
Sulfur, wt.%
PCBs
* Table A-2 identifies the source of analytical data for each used oil sample. Table A-3 provides
odes for each sanple number which describe the specific generating source of used oil and the end-use.
A-13
0240
-------
ANALYTICAL DATA TOR USED OIL SAMPLES
Sample Number*
93
345
-
94
356
153
95
"zl.
-
96
2B
-
97
33
-
98
33
-
_ g? TOO Tt
SIC 345 356 28. 2B 33 33 33 33 3
Flash Poinc (°F) 155 290 - .
Metals
Arsenic ------__.
Aluminum _________
Barium - 55 23 25 10 75 0
Beryllium - - - - - - - - -
Cadmium 14 0.1 3 3 0 0 3 5
Chromium - 0.01 1 21 4 5 25 18
Cobalt .---.-...
Copper 6.7 0.6 1 460 11 32 20 1
Iron - 12 1.750 5 950 1,000 5,100
Lead 3.6 0.6 7 300 37 25 22 28
Magnesium ____---,-
Manganese -- 025----
Molybdenum ________
Nickel ________
Jeleniur. ________
Silicon - - 2 70 2 250 100 6
Silver ________
Sodium ________
Tin ________
Titanium ________
Vanadium ________
Zinc 123 0.7 25 5,000 5 500 8 92
Volatile Organics
Dichlorodifluoromethane ________
Tncnlorotnfluoroethane ________
1,1,1-Trichloroethane ________
Trichloroethylene ________
Tetrachloroethylene ________
Phenol ___•_____
Benzene ________
Toluene ________
Ethyl Benzene ________
Xylenes ________
Mechylene Chloride ________
PNAs
Naphthalene ________
Phenanthrene/Anthracene --------
Pyrene ________
Benzo(a)anthracene ________
Benzo(a)pyrene ________
Alkylbenzene (CgHjo) ________
Alkylnaphthalene (C.-H.,) -
Phosphorus - 0 2.500 ' 10 425 800 600
Chlorine, wt £ ________
Sulfur, wt „ 0.90 0.79 ------
PCBs ________
* Table A-2 identifies the source of analytical data for each used oil sample. Table A-3 provides
codes for each sample number which describe the specific generating source of used oil and the end-use.
A-14
-------
TABLE A-l (continued)
ANALYTICAL DATA FOR USED OIL SAMPLES
Sample Number *
105
34
300
106
34
350
107
35
210
108
37
109
480
110
440
102 103 104
SIC 33 33 34
Flash Point (°F) 200
Metals
Arsenic -----___
Aluminum .-.--_ 2,000 7 7
Barium 70 15 70 0 10 0 190 10 0
Beryllium _______--
Cadmium 053010- 00
Ororciun 3 3 18 3 5 1 9 4 7
Cobalt ___--__--
Copper 1 60 380 10 20 0 -
Iron 13 120 700 18 60 12 375 33 55
Lead 2 55 2,000 5 8 1 78 17 10
Magnesivir. __-------
Manganese _-- 430- 10
Molybdenum __-------
Nickel ___------
Selenium __-------
Silicon 5 16 110 7 10 1 2,500 8 10
Silver ___------
Sodiun __-------
Tin ____._--_
Titanium ___------
Vanadium __-------
Zi.; 2 20 450 i 8 1 250 1 50C
Volatile Organics
Dichlorodif luorone thane __-------
Trichlorof luoromethane ___------
Trichlorotrifluoroethane _ ___-----
1,1,1-Trichloroethane ___------
Trichloroethylene - - - ~ ~ . ~
Phenol __-------
Benzene - ~-~ ~ ~ •* ~ ~ ~
Toluene ____-----
Echyl Benzere «.__------
Xyler.ar __-------
Methylene Chloride ______---
PNAs
Naphthalene - - - ~ ~ " ~ ~ . ~
Phenanthrene//j\thracene ____-----
Pyrene ___------
Benzo(s) anthracene ___------
Benzo(a)pyrene „__------
Alkylbenzene (CgH, ) __-_-----
Alkylnaphthalene tt. ,H, ,) -
Phosphorus 1Z iZ 0 40 400 0 10 0 700 10 450
Chlorine, wt!; _____----
Sulfur, wt% _____----
PCBs _.__-----
* Table A-2 identifies the source of analytical data for each used oil sample. Table A-3 provides
codes for each sample number which describe the specific generating source of used oil and the end-use.
A-15
0241
-------
TABLE A-l (continued)
ANALYTICAL DATA FOR USED OIL SAMPLES
Sample Number*
111
37
445
112
37
410
113
356
150
114
34
225
115
356
-
116
352
150
117
34
150
118
345
150
SIC
Flash Point (°F)
Metals
Arsenic ______
Aluminum 36 4 - - - _ _ _
Barium 10 550 ---__.
Beryllium ------__
Cadmium 0 0 0 0.6 0.2 0.1 0.3 0.4
Chromium 3 5 00.3 10 3 705
Cobalt ------- i
Copper - 1 0.3 5 12 11 4
Iron 20 13 -
Lead 780 30 4 2.3 84 17 126 8
Magnesium -----___
Manganese 00-----.
Molybdenum -----___
Nickel -----___
Selenium --------
Silicon ' 4 12 -
Silver ---___ __
Sodium ---___ __
Tin ----____
Ticaniua -----___
Vanadium --____ __
Zinc 420 270 28 23 90 38 50 51
Volatile Organics
Dichlorodifluoromethane -----.._
Trichlorofluoromethane --------
Trichlorotrifluoroethane ------__
1,1,1-Trichloroethane -----___
Trichloroethylene - - - - - - _ • _
Tetrachlctoethylene --__-___
Phenol - - - _ _ - _
Benzene -----___
Toluene _----__-
Ethyl Benzene --------
Xylenes --------
Methylene Chloride --------
PNAs
Naphthalene --------
Phenanthrene/Anthracene --------
Pyrene ----____
Benzo(a)anthracene --------
Benzo(a)pyrene --------
Alkylbenzene (C9H12) --------
Alkylnaphthalene (C..H.-) --------
Phosphorus 300 100 --____
Chlorir.e, wtX ----____
Sulfur, wt % - - 0.0 0.4 - 0.1 0.02 0.02
PCBs --------
* Table A-2 identifies the source of analytical data for each used oil sample. Table A-3 provides
codes for each sample number which describe the specific generating source of used oil and the end-use.
A-16
-------
TA3LE A-i (.continued;
ANALYTICAL DATA FOR USED OIL SAMPLES
Sample Number*
SIC
Flash Point ( «F)
Metals
Arsenic
A ] umir.um
Barium
Beryllium
Cadmium
Chromium
Cobalt
Copper
Iron
Lead
Magnesium
Manganese
Molybdenum
Nickel
Seler.ivn
Silicon
Silver
Sodium
Tin
Titanium
Vanadium
Zinc
119
3312
475
_
12
23
-
2
45
-
140
1,500
19
6
21
2
44
-
9
0.2
9
5
4
1
4
120
3519
525
_
1
5
-
0
4
-
4
35
90
1
1
1
4
-
1
0.2
0
45
0
2
1
121
3312
315
_
1
45
-
0
2
-
3
18
7
0
0
0
3
-
11
0.1
0
0
0
1
39
122
3312
470
_
3
13
-
0
8
-
3
120
150
4
12
1
5
-
5
0.1
0
5
0
2
10
123
3451
-
_
1
11
-
0
4
-
0
68
4
11
3
2
4
-
4
0.1
0
0
1
1
14
124
3714
280
_
6
76
-
1
5
-
16
240
230
74
95
1
5
-
29
0.2
97
5
2
2
39
125
3452
330
_
3
330
-
19
4
-
11
36
100
3
1
1
4
—
6
0.2
0
5
22
4
530
126
3522
235
,
^
9
55
-
0
15
-
27
24
31
13
11
1
10
-
680
0.2
25
2
2
11
30
127
3462
195
_
65
40
-
1
18
-
25
1,000
170
20
250
2
29
-
650
0.6
40
7
110
5
23
Volatile
Dichlorodifluoromethane
Trichlorofluoroaethane
Trichlorotri fluoroethane
1,1,1-Trichloroethane
Trichloroethylene
Tetrachloroethylene
Phenol
Benzene
Toluene
Ethyl Benzer e
Xylenes
Metnylene Chloride
PNAs
Naphrt alene
Phenanthrene/Anthracene
Pvrene
Benzo(a)anthracene
.Benzo(a)pyrene
Alkyloenzene (CgH^)
Alkyinaphthalene (C.-H,.)
Phosphorus "
Chlorine, wt Z
Sulfur, wt '.'
PCBs
340
10
90
50
19
0.4
0.2
0.6
2,000
0.2
360
0.8
50
0.2
960
0.3
* Table A-2 identifies the source of analytical data for each used oil sample. Table A-3 provides
codes for each'sample number which describe the specific generating source of used oil and the end-use.
A-17
0242
-------
TABLE A-l (continued)
ANALYTICAL DATA FOR USED OIL SAMPLES
, . - — •
Sample Number*
SIC
Flash Point CD
Metals
Ar senic
Aluminum
Barium
Beryllium
Cadmium
Chromium
Cobalt
Copper
Iron
Lead
Magnesium
Hangar.es e
Molybdenum
Nickel
Selenium
Sllicori
Silver
Sodium
Tin
Titanium
Vanadium
Zinc
128
3452
280
.
30
10
-
1
1
-
3
110
17
11
17
0
10
~ 20
0.1
10
0
1
0
7
129
3741
355
_
4
15
-
1
5
-
120
900
24
19
9
0
7
_
19
0.5
7
5
1
1
200
130
3452
325
_
3
10
-
0
9
-
6
27
27
6
64
0
4
_
^
0.1
0
0
0
1
3
131 132 133
3522 35 34
220 80 150
_ _ —
22 -
100
1 7 0.6
14 0.2 2
_
34 4 39
170
700 49 23
55 -
17 -
1 -
12 -
37 -
0.3
33 -
5 -
5 -
15 -
100 174 187
134
34
150
_
„. .
_
_
0.4
3
„
91
13
—
_
„
—
_
_
_
_
—
—
«.
216
Volatile Organics
Dichlorodifluoromethane
Trichlorofluoromethane
Trichlorotrifluoroethc.ne
1,1,1-Trichloroethane
Trichloroethylene
Tetrachloroethylene
Phenol
Benzer.fc
Toluene
Ethyl Benzene
Xylenes
Methylene Chloride
PSAs
Naphthalene
Phenanthrene/Anthracene
Pyrene
Benzo(a)anthracene
Benzo(a)pyrene
Alkylbenzene
Alkylt-phthalere
Phosphorus
Chlorine, wt %
Sulfur, «t %
PCBs
70
0.4
300
0.3
57
0.4
350
0.6
0.90
0.21
0.30
* Table A-2 identifies the source of analytical data for each used oil sample. Table A-3 provides
codes for each sample number which describe the specific generating source of used oil and the end-use.
A-18
-------
TABLE A-l (continued)
ANALYTICAL DATA FOR USED OIL SAMPLES
Flash Point (°F)
Metals
Arsenic
Aluminum
Barium
Beryllium
Cadmium
Chromium
Ccoalt
Copper
Iron
Lead
Magncsiin.
Manganese
Molybdenum
Nickel
Selenium
Silicon
Silver
Sodium
Tin
Titanium
Vanadium
Zir.;
135
_
-
17
36
-
3
14
-
24
170
260
0
1
10
0
-
16
0
20
8
7
25
330
136
.
-
12
36
-
4
31
-
6
190
7
90
124
1
21
-
44
0
370
10
1
5
6
137
370
—
8
34
4
-
10
-
12
100
15
26
6
1
0
-
32
0
25
6
0
8
12
Sample
138
-
—
3
220
4
-
5
-
3
6
4
1
3
1
0
-
2
0
12
7
0
6
200
Number*
139
270
™"
3
7
-
5
1
-
12
18
8
1
6
1
0
-
2
0
1
8
0
0
190
140
200
*
5
13
-
3
7
-
10
21
3
2
4
9
0
-
33
0
1
3
1
9
47
141
385
™
3
1
-
4
5
-
3
2
4
3
3
1
0
—
2
0
1
3
0
6
580
142
170
™
3
45
-
1
16
-
9
31
11
3
7
2
0
-
63
0
19
6
1
19
36
Volatile Organics
Dichlorodiflucromethane
Trichlorofluoromethane
Trichlorotrifluoroethane
1,1,1-Trichloroethane
Trichloroethylene
Tetrachloioeth)It re
Fhenol
Benzene
Toluene
Ethyl Benzene
Xylenes
Methylene Chloride
PNAs
Naphthalene
Fhenanthrene/Anthracene
Pyrene
Benzo(a)anthracene
Benzo(a)pyrene
Alkylbenzene (C9Hi2)
Alkylnaphthalene
Phosphorus
Chlorine, wt '/'.
Sulfur, wt ','.
390
0.50
13
0.10
58
0.20
58
0.50
15
0.30
13
0.40
210
0.40
70
0.50
* Table A-2 identifies the source of analytical data for each used oil sample. Table A-3 provides
codes for each sample number which describe the specific generating source of used oil and the end-use.
A-19
0243
-------
TABLE A-l (continued)
ANALYTICAL DATA FOR USED OIL SAMPLES
Flash Point (°F)
Metals
Arsenic
Aluminum
Barium
Beryllium
Cadmium
Chromium
Cobalt
Copper
Iron
Lead
Magnesium
Manganese
Molybderum
Nickel
Seler.iu-
Siiicon
Silver
Sodium
Tin
Titanium
Vanadium
Zinc
143
440
-
3
10
-
8
3
-
16
1
0
4
3
0
0
-
2
0
4
3
0
3
56
144
.
-
36
35
-
7
8
-
1,160
200
23
45
16
19
27
-
62
0.1
1
40
1
4
1,100
145
410
-
24
120
-
8
16
-
140
85
1,400
1,000
9
2
0
-
? -i
L t.
0
85
25
0
8
760
Sample Numbers*
146 147 148 149
415 -
_
2 -
5 -
-
4 0.7 - 2.5
3 1.2 - 0.1
-
7 5.9 - 9.3
2 - 10,000
4 51 0.6
0 -
3 -
1 -
0 1.2 - 0.4
- - _ _
2 -
0 -
1 -
1 -
0 -
3 -
600 150 - 0.8
* •"
150 1
_ _
-
_ _
_ _
<0.
- 0.
0.
_ _
8 0.
_ _
0.
-
_
_
2.
..
_
.»
_
_
_
_
8
Volatile Organics
Dichlorodifluoromethane
Trichlorofluoromethane
Tricl lorotrifluoroethane
1,1,1-Trichloroethane
Tr ichlo roethylene
Tetrachloroethylene
Phenol
Benzene
Toluene
Ethyl Benzene
Xylenes
Methylene Chloride
PNAs
Naphthalene
Phenanthrene/Anthracene
Pyrene
Benzo(a)anthracene
Benzo(a)pyrene
Alkylbenzene (C9Hi2)
Alkylnaphthalene (C..H.,)
Phosphorus
Chlorine, wt 2
Sulfur, wt 2
PCBs
52
13
28
21
62
0.40
1,080
0.10
400.
0.40
200
0.40
<50
* Table A-2 identifies the source of analytical data for each used oil sample. Table A-3 provides
codes for each sample number which describe the specific generating source of used oil and the end-use.
A-20
-------
TABLE A-l (continued)
ANALYTICAL DATA FOR USED OIL SAHPLES
Sample Number*
Flash Point (°F)
Metals
Arsenic
Aluminum
Barium
Beryllium
Cadmium
Chromium
Cobalt
Copper
Iron
Lead
Magnesium
Manganese
Molybdenum
Nickel
Selenium
Silicon
Silver
Sodium
Tin
Titanium
Vanadium
Zinc
152 153 154
380
_
33 -
120
-
3 <0.01
28 <0.01
_
150 13
520
15 21
42 -
17 -
_
5 <0.01
_
90 -
0 -
180
21 -
0 -
_
12 14
155
270
-
3
7
-
5
1
-
12
18
8
1
6
1
0
-
2
0
1
8
0
0
190
156 157
102
<0.01 <0.01
-
-
7
4 0.2
520 2.5
.
96 42
-
3,500 114
-
-
-
300 4
-
-
30
-
-
-
-
43 324
158
_
39
_
_
21
7
_
15
18
50
11
20
16
4
-
22
0
400
140
21
7
160
159
•' —
_
_
<0.01
0.22
0.24
_
0.08
_
0.01
-
.
-
0.12
.
_
-
-
_
-
-
1.2
160
_
3
220
_
4
5
_
3
6
4
1
3
1
0
-
2
0
12
7
0
6
200
Volatile Orgar.ics
Dichlorodifluoromethane
Trichlorofluoromethane
Trichlorotrifluoroethane
1,1,1-Trichloroethane
Trichloroethylene
Tetrachloroethylene
Phenol
Benzene
Toluene
Ethyl Benzene
Xylenes
Met.rr. lene Chloride
PSAS
Naphthalene
Phenanthrene/Anthracene
Pyrene
Benzo(a)anthracene
Senzo(a)pyrene
Alicylbenzene (C^Hi^)
AlKylnaphthalene tc.,H.-)
Phosphorus X
Chlorine, wt 1
Sulfur, wt 7.
PCBs
300,000
100.000
15
0.3
0.3
190
0.09
<0.5
270
0.1
42
0.01
0.4
7
58
0.5
* Table A-2 identifies the source of analytical data for each used oil sample. Table A-3 provides
codes for each sample number which describe the specific generating source of used oil and the end-use.
A-21
0244
-------
TABLE A-l (continued)
ANALYTICAL DATA FOR USED OIL SAMPLES
Flash Point (°F)
Metals
Aluminum
Arsenic
Barium
Beryllium
Cadmium
Chromium
Cobalt
Copper
Iron
Lead
Magnesium
Manganese
Molybdenum
Nickel
Selenium
Siliccr.
Silver
Sodium
Tin
Titanium
Vanadium
Zinc
Volatile Organics
Dichlorodif luororae thane
Trichlorofluorome thane
Trichlorotrifluoroe thane
1,1, 1-Tr ichlor oe thane
Trichloroethylene
Tetrachloroethylene
Phenol
Benzene
Toluene
Ethyl Benzene
Xylenes
Methylene Chloride
PKAs
Naphthalene
Phenan thr ene /Anthracene
Pyrene
Benzo( a) anthracene
Benzo(a)pyrene
Alkylbenzene (C-H.-)
Alkylnaphthalene *Ci2H12^
Phosphorus
Chlorine, wt. 5
Sulfur, wt. %
PCBs
Sample Number*
161 162 163 164 165 166 167
340 405 >147 >147 >147 >147 >147
<100 >100 <5 <5 <5 <5 <5
_---___
160 150 150 240 240
__--___
<10 <10 <10 <10 10
5.0 2.0 -
_______
10.0 5.0 218 96 149 192 187
>200.0 34.0 3,860 1,500 2,650 3,590 2.680
38.0 >100.0 284 189 264 275 311
-------
-------
24 <5 11 12 10
- 37 11 18 20 16
<5 <5 <5 <5 <5
2i.O 7.0 -
<1.0 <1.Q <5 <5 <5 <5 <5
10.0 7.0 -
9.0 <1.0 -
_______
56 33 45 52 35
598 381 646 1.080 831
_______
_______
_______
2,600 380 880 250 410
240 <200 <200 <200 320
2.200 560 780 1,100 1,200
_______
_______
______
_______
_______
-------
•
-
-------
-------
_____--
-------
— — — — — — —
-------
0.83 <0.1 0.32 0.12 0.14 0.22 0.21
0.71 0.54 0.28 0.34 0.29 0.34 0.33
168
>147
<5
„
140
-
10
_
_
104
1,650
217
-
-
7
8
<5
-
<5
-
-
—
29
706
-
-
-
<200
<200
740
_
_
-
-
-
-
-
-
-
—
—
—
—
0.13
0.38
* Table A-2 identifies the source of analytical data for each used oil sample. Table A-3 provides
codes for each sample number which describe the specific generating source of used oil and the end-use.
A-22
-------
TABLE A-l (continued)
ANALYTICAL DATA FOR USED OIL SAMPLES
Flash Point (°F)
Metals
Aluminum
Arsenic
Barium
Beryllium
Cadmium
Chromium
Cobalt
Copper
Iror.
Lead
Magnesium
Manganese
Molybdenum
Nickel
Selenium
Silicon
Silver
Sodium
Tin
Titanium
Vanadium
Zinc
Volatile Organ ics
Dichlorcdif luor one thane
Tricniororlucr one thane
Trichlorotrifluoroethane
1,1, 1-Trichloroethane
Trichloroethylene
Tetrachloroethylene
Phenol
Benzene
Toluene
Ethyl Benzene
Xvlenes
Methylene Chloride
PNAs
Naphthalene
Phenanthrene /Anthracene
Pyrene
3enzo(a)anthracene
Benzo(a)pyrene
Alkylbenzene (CgH ,)
AlkylnaphthalenI tc.-lL-)
Phosphorus
Chlorine, wt. %
Sulfur, wt. %
PCBs
169
>147
-
<5
150
-
20
-
_
1,040
1,470
268
-
-
6
8
<5
-
<5
-
-
-
21
469
-
-
-
1,900
460
870
-
-
-
-
-
-
-
-
-
-
-
-
-
-
0.32
0.37
<10
170
>147
-
<5
320
-
30
-
_
317
4,900
603
-
-
16
30
<5
-
<8
-
-
-
79
2,380
-
-
-
<200
<200
<200
-
-
-
-
-
-
-
-
-
-
-
-
-
-
0.18
0.55
<10
171
>147
-
<5
440
-
<10
-
-
147
1,770
237
-
-
7
15
<5
-
<8
-
-
-
32
895
-
-
-
260
220
3,800
-
-
-
-
-
-
-
-
-
-
-
-
-
-
0.62
0.38
<10
Sample Number*
172 173
>147 >147
-
<5 <5
430
-
20
-
- _
339
4,840
591
-
-
19
33
<5
-
<8
-
-
-
92
1,310
-
-
-
1,200
430
1.600
- -
-
-
-
-
-
-
-
-
-
-
— —
— —
— — •
0.30 -
0.35 -
<10
174
>147
-
<5
90
-
<10
-
_
98
2,470
156
-
-
<5
19
<5
-
<8
-
-
-
47
277
-
-
-
3,500
15,000
710
-
-
-
-
-
-
-
-
-
-
-
—
—
—
1.21
0.30
<10
175
>147
-
<5
190
.
40
-
_
168
2,280
419
-
-
8
13
<5
-
<8
-
-
_
36
831
-
-
-
3,100
1,600
370
-
-
-
-
-
-
-
-
-
-
-
—
•
~
0.21
0.24
<10
176_
>147
-
<5
240
-
<10
_
»
145
1,490
269
-
-
7
11
<5
_
<8
-
-
_
26
722
-
-
-
310
240
990
-
-
-
-
-
-
-
-
-
-
-
—
—
—
0.2
0.39
<10
* Table A-2 identifies the source of analytical data for each used oil sample. Table A-3 provides
cooes for each sample number which describe the specific generating source of used oil and the end-use.
A-23
024
-------
TABLE A-l (continued)
ANALYTICAL DATA FOR USED OIL SAMPLES
Sample Number and Description*
Flash Point (°F)
Metals
Arsenic
Aluminum
Barium
Beryllium
Cadmium
Chromium
Cobalt
Copper
Iron
Lead
Magnesium
Manganese
Molybdenum
Nickel
Selenium
Silicon
Silver
Sodium
Tin
Titanium
Vanadium
Railroad
Drainings
177
1.83
1.46
1.92
1.6
11.9
0.8
4.8
27.9
12.5
Recipro.
Engine Oil
178
Jet Engine
Oil
179
14
33
3,187
9
28
19
Volatile Organics
Dichlorodifluoromethane
Trichlorofluoromethane
Trichlorotrifluoroethane
1,1,1-Trichloroethane
Trichloroethylene
Tecrachloroethylene
Phenol
Benzene
Toluene
Ethyl Benzene
Xylenes
Methylene Chloride
PNAs
Naphthalene
Phenanthrene/Anthracene
•Pyrene
Benzo(a)anthracene
Benzo(a)pyrene
Alkylbenzene (CgH,,)
Alkylnaphthalene (C^H^)
Phosphorus
Chlorine, wt %
Sulfur, vt "
PCBs
22.5
* Table A-2 identifies the source of analytical data for each used oil sample. Table A-3 provides
codes for each sample number which describe the specific generating source of used oil and the end-use.
A-2i
-------
e
o
•H
0) 4J
• CO />~\
s
PL, c a
u
g
en oo
CO 55
ts
a)
3
C
O
u
I
C/5
Dfi
£
H
a
g
•H
CO *J
- 18 /-v
ea * E
U J-i C.
Q> -
U
g
v v
co
o
T-I
W 4J
8
^ e
•u a
e a
CU v-'
u
g
u
oo
ca fi
OH O.
I 024G
A-25
-------
TABLE A-l (continued)
ANALYTICAL DATA FOR USED OIL SAMPLES
Sample Number*
Flash Point (°F)
Metals
Aluminum
Arsenic
Barium
Beryllium
Cadmium
Chromium
Cobalt
Copper
Iron
Lead
Magnesium
Manganese
Molybdenum
Nickel
Selenium
Silicon
Silver
Sodium
Tin
Titanium
Vanadium
Zinc
Volatile Organics
Dichlorodifluorome thane
Trichlcrrcluoro-.e thane
Trichlorotr if luoroe thane
1,1,1-Trichloroe thane
Trichlcjroethylene
Tetrachloroethylene
Phenol
Benzene
Toluene
Ethyl Benzene
Xy lanes
Methylene Chloride
PNAs
Naphthalene
Phenanthrene /Anthracene
Pyrene
Benzo (a) anthracene
Benzo(a)pyrene
Alkylbenzene (CQH17)
AlkylnaphthalenI tC. ,H. ,)
Phosphorus
Chlorine, wt. 2
Sulfur, wt. %
PCBs
237
186
8.4
9
68
0.04
1.5
3.4
0.2
31
130
1,300
93
6.2
2.4
2.1
<0.5
11
<0.02
55
110
0.1
1.0
830 ;
<20
<20
160
1,700
570
530
<10
110
5,000
1,200
-
<20
780
350
50
30
20
^
-
0.26
0.72
238
200
8.0
100
44
0.02
1.4
2.9
<0.06
32
120
1,250
190
5.2
1.6
1.1
<0.5
20
<0.02
85
5.5
0.1
<0.1
1,100
<20
<20
<20
910
<20
650
<10
90
2,400
540
1,300
<20
-
330
150
30
20
<10
23,000
-
0.18
1.2
<0.5
239
194
15
11
44
0.03
1.3
5.7
<0.07
30
180
1,420
350
11
4.4
1.7
<0.5
22
<0.02
140
8.5
0.5
<0.1
940
<20
360
1,350
210
<20
270
<10
120
970
300
1,070
<20
110
40
10
-------
TABLE A-l (continued)
ANALYTICAL DATA FOR USED OIL SAMPLES
Sample Number*
Flash Point (°F)
Metals
Arsenic
Aluminum
Barium
Beryllium
Cadmium
Chromium
Cobalt
Copper
Iron
Lead
Magnesium
Har.garese
MclvDaenum
Nickel
Selenium
Silicon
Silver
Sodium
Tin
Titanium
Vanadium
Zinc
246 24I_
<10 370
60 120
241
40
50
243
40
50
2*0
80
40
211
~120
50
252
30
70
25i
~ 50
80
60
10
10
10
10
10
10
40
680
90
10
10
<10
100
1.360
800
200
20
50
50
10
150
300
160
10
<10
10
10
150
290
160
10
<10
10
10
670
160
250
40
<10
20
20
980
310
350
60
10
30
20
180
1,780
340
10
10
<10
40
200
1.380
190
10
<10
<10
10
80
20
580
530
460
100
40
550
80
360
60
390
80
400
60
400
250
190
110
170
370
600
10
140
210
110
160
10
1.080
140
140
990
Dichlorodifluoromethane
Trichlorof lucroir.e thane
Trichlorotrifluoroethane
1,1.1-Trichloroethane 2,260
Trichloroethylene 150
Tetrachloroethylene 190
Pher.cl
Benzer.e
Toluene
Ethyl Benzene
Xylenes
Methylene Chloride
PNAs
Naphthalene
Phenanthrene/Anthracene
Pyrene
Bento(a)anthracene -
Benzo(a)pyrene
Alkylbenzene (CgHj^) -
Alkylnaphthalene (C.-H.,)
Phosphorus iZ 1,750
Chlorine, wt Z
Sulfur, wt Z
PCBs "<50
1,740
<50
510
<50
500
<50
280
<50
250
<50
1,110
<50
1,130
<50
* Table A-2 identifies the source of analytical data for each used oil sample. Table A-3 provides
codes for each sample number which describe the specific generating source of used oil and the end-use.
A-2 7
0247
-------
TABLE A-l (continued)
ANALYTICAL DATA FOR USED OIL SAMPLES
Sample Number*
-J-i 23i __57
Flash Point (°F) ------__
Metals
Arsenic ----____
Aluminum -----___
Barium ----___ 2-1,630
Beryllium _--_____
Cadmium <5 <10 <10
-------
TABLE A-l (continued)
ANALYTICAL DATA FOR USED OIL SAMPLES
Flash Point (°F)
Metals
Arsenic
Aluminum
Barium
Beryllium
Cadmium
Chromium
Cobalt
Copper
Iron
Lead
Magnesium
Manganese
Molybdenum
Nickel
Selenium
Silicon
Silver
Sodium
Tin
Titanium
Vanadium
Zinc
262 261 2&i
385
_ -
5.8
•el
_
_
0.7
_
2.5
6
20
0.4
_
_
_
_
- - 305
_
106
_
_
_
12.0
Sample Number*
265 266
199 450
-
6.8
<1
-
-
18.2
- -
34.0
14.0
2.140
160
-
-
-
-
309.0
-
12.0
- -
-
-
874
JU
_
<25
-
<25
<2.5
<5
170
_
340
1.040
53
-
13
.
89
<25
-
6.4
1,300
-
<20
-
72
16J, 269
- -
.>
<25
-
<25
<2.5
<5
86
_ _
92
390
39 80
-
4
-
19
<25
-
<5
140
- —
<20
_ -
64
2m
_
_
-
_
-
_
_
_
_
-
IOC
-
-
-
_
-
_
-.
-
.
-
_
-
Volatile Organics
Dichlorodifluorotnethane
Trichlorofluoromethane
Trichlorotrifluoroethane
1,1,1-Trichloroethane
Trichloroethylene
Tetrachloroethylene
Phenol
Benzene
Toluene
Ethyl Benzene
Xylenes
Mechylene Chloride
PNAs
Naphthalene
Phenanthrene/Anthracene
Pyrene
Benzo (a)anthracene
' Benzo(a)pyrene
Alkylbenzene (C9H12)
Alkylnaphthalene (C,,H--)
Phosphorus
Chlorine, wt %
Sulfur, wt %
PCBs
550,000
80,000
110,000
110,000
7,100 1,400
200 1,700
280 1,200
20
360
680
300
350
1,800
130
310
70,000 139,000
920
220
1,600
270
75
0.43
22.0
0.20
860
* Table A-2 identifies the source of analytical data for each used oil sample. Table A-3 provides
codes for each sample number which describe the specific generating source of used oil and the end-use.
A- 2 9
0248
-------
TABLE A-l (continued)
ANALYTICAL DATA FOR USED OIL SAMPLES
Sample Number *
21L 222. 211 274 27J 276 277 278
Flash Point (°F) ________
Metals .
Arsenic _ •>
Aluminum ________
Barium ________
Beryllium ________
Cadmium ________
Chromium ---_-___
Cobalt --_-____
Copper ________
Iron ________
Lead 50 40 730 410 1,100 <10 30 370
Magnesium ________
Manganese ________
Molybdenum ________
Nickel ________
Selenium ________
Silicon ________
Silver - - - ' -
Sodium ________
Tin ________
Titanium ________
Vanadium ________
Zinc ________
Volatile Organics
Dichlorodifluoromethane 8 <5 210 360 26 <5 <5 2,000
Trichlorofluoromethane ________
Trichlorotrifluoroethane ----____
1,1,1-Trichloroe thane 640 59 540 1,300 480 80 <5 2,500
Trichloroethylene 25 13 160 370 830 <5 5 410
Tetrachloroethylene 54 22 260 1,200 280 64 5 1,500
Phenol ________
Benzene ________
Toluene ________
Ethyl Benzene - _-_ _ _ _ _ _
Xylenes ________
Methylene Chloride <5 <5 30 100 50 <5 <5 1,000
PNAs
Naphthalene _---____
Phenanthrene/Anthracene ________
Pyrene ________
Benzo(a)anthracene - - - - - - --
Benzo(a)pyrene ________
Alkylbenzene
Alicylnaphthalene
Phosphorus
Chlorine, wtX
Sulfur, wtX
PCBs
* Table A-2 identifies the source of analytical data for each used oil sample. Table A-3 provides
codes for each sample number which describe the specific generating source of used oil and the end-use.
A-30
-------
TABLE A-l (continued)
ANALYTICAL DATA FOR USED OIL SAMPLES
Sample Number*
281 _£_. i__: .284 221 286 287 288,
Flash Point (°F)
Metals
Arsenic
Aluminum
Barium
Beryllium
Chromium ___- _____
Cobalt _---___-_
Copper ____ _____
Iron _________
Lead 990 920 900 670 <10 190 1,200 980 <10
Magnesiur. _ _ _ _ --.-_
Manganese ____ _____
Molybdenum - - -.- _ - - _ _
Nicicel - - - . -
Selenium ____ _____
Silicon _________
Silver - - - - - - ' -
Sodium ____ _____
Tin _________
Titanium ____ _____
Vanadium ____ _____
Volatile Organics
Dichiorodifluoromethane 220 1,500 <5 5 9 <5 54 1,300 <5
Trichlorof luoromethane _________
Trichlorotrifluoroethane _________
1,1,1-Trichloroethane 1,300 1,100 10 26 76 <5 120 3,300 380
Trichloroethylene 660 400 <5 <5 <5 <5 57 2,900 110
Tetrachloroethylene 710 650 10 14 29 <5 150 1,500 92
Phenol ____ _____
Benzene ____----_
Toluene - - ~ -
Ethyl Benzene _________
Xyleaes ___- _____
Methylene Chloride 200 100 <5 <5 <5 <5 <5 5,000 1,000
PNAs
Naphthalene _________
Phenanthrene/ Anthracene _________
Pyrene _________
Benzo(a)anthracene -.-
Benzo(a)pyrene _________
Alkylbenzene (C9H12) -_-------
Alkylnaphthalene CC
Phosphorus
Chlorine, wtZ
Sulfur, wt%
PC3s
* Table A-2 identifies the source of 'analytical data for each used oil sample. Table A-3 provides
codes for each sample number which describe the specific generating source of used oil and the end-use.
A-31
0249
-------
8
TABLE A-l (continued) *
ANALYTICAL DATA FOR USED OIL SAMPLES
Sample Number*
283 220. -UiL 292 193 294 295 1__;
Flash Point (°F) ---__-__
Metals
Arsenic ________
Aluminum ________
Barium ________
Beryllium __-._,.___
Cadmium _••_____.
Chromium " -
Cobalt ________
Copper - - - -.-
Iron ________
Lead 600 480 420 520 380 360 680 10
Magnesium --_-____.
Manganese - - - - - - -.-
Molybdenum ________
Nickel _____-_.
Selenium ________
Silicon ________
Silver ________
Sodium ________
Tin ________
Titanium ________
Vanadium ________
Zinc ________
Volatile Organics
Dichlorodifluoromethane <5 19 130 180 1,700 74 <5 <5
Trichierofluoromethane ________
Trichlorotrifluoroethane ________
1.1,1-Trichloroethane <5 310 1,200 1,300 1,700 360 130 <5
Trichloroethylene <5 550 500 760 1,400 200 <5 <5
Tetrachloroethylene <5 1,000 900 618 1,300 200 • 110 <5
Pheacl -•-
Benzene ________
Toluene _ ___ _ - - - -
Ethyl Benzene --_-____
Xvlenes ________
Methyler.e Chloride <5 <5 300 500 4,000 5,000 100
PNAs
Naphthalene ----____
Phenanthrene/Anthracene ---_____
Pyrene ________
Benzo (a)anthracene ________
Benzo(a)pyrene ________
Alkylbenzene
Alkylnaphthalene
Phosphorus
Chlorine, wtX
Sulfur, utZ
PCBs
* Table A-2 identifies the source of analytical data for each used oil sample. Table A-3 provides
codes for each sample number which describe the specific generating source of used oil and the end-use.
A-32
-------
TABLE A-l (continued)
ANALYTICAL DATA FOR USED OIL SAMPLES
Sample Number*
298 299 1°P_ 101. 102 303 304 305
306
Flash Point (°F) _--__-__-
Metals
Arsenic _________
Aluminum ___-____-
Barium _________
Beryllium .________-
Cadmium _________
Chromium _________
Cobalt _----____
Copper _-_---__-
Iron ---------
Lead 100 1,400 700 320 390 <10 <10 830 10
Magnesium - - --
Manganese ___----_-
Molybdenum _________
Nickel _-__--__-
Selenium - - - - - - - _._
Silicon ___--_-_-
Silver ---------
Sodium _-_-----_
Tin _________
Titanium _________
Var.3ciu- _________
Zinc _-__-_--_
Volatile Organics
Dichlorodifluoromethane 380 120 2,200 8 860 <5 <5 100 20
Trichlorofluoromethane ___--_-_-
Trichlorotrifluoroethane
1,1,1-Trichloroethane 1,700 920 440 570 1,400 <5 <5 480 150
Trichloroethylene 130 1,100 8iO 90 1,600 <5 <5 180 2-
Tetrachloroethylene 310 1,200 200 250 1,300 <5 <5 330 :.
Phenol - - _ -
Benzene ___----_-
Toluene ____-_-_-
£tnyl Senzene _________
Xylenes __-_-----
Methylene Chloride - 300 600 30 600 <5 <5 - <5
PNAs
Naphthalene _________
Phenanthrene/Anthracene -_______-
Pyrene ____---_-
Benzo(a)anthracene _________
Benzo(a)pyrene _________
Alkylbenzene
Alkylnaphthalene
Phosphorus
Chlorine, wtX
Sulfur, wt%
PCBs
* Table A-2 identifies the source of analytical data for each used oil sample. Table A-3 provides
codes for each sample number which describe the specific generating source of used oil and the end-use.
A-33
0250
-------
TABLE A-l '(continued)
ANALYTICAL DATA FOR USED OIL SAMPLES
Sample Number*
307 _306 309 310 311 312 313 314
Flash Poinc (°F) - - ______
Metals
Arsenic - ~ ______
Aluminum - - ______
Barium -- ______
Beryllium - - ______
Cadmium -- ______
Chromium ________
Cobalt ________
Copper -- ______
Iron ________
Lead 10 60 230 <10 220 70 <10 220
Magnesium -- ______
Manganese -- ______
Molybdenum -- ______
Nickel ________
Selenium ________
Silicon -- ______
Silver - - ______
Sodium -- ______
Tin ________
Titanium ________
Vanadium ________
Zinc ________
Volatile Organics
Dichlorodifluoronethane 58 20 160 20 980 2,000 <5 300
Trichlorof luorotnechane ________
Trichlorotrifluoroethane --------
1,1,1-Trichloroethane 370 320 640 150 1,200 1,800 <5 1.100
Trichloroethylene 75 46 1,100 96 7,000 1,400 <5 880
Tetrachloroethylene 230 190 1,700 99 370 3,900 <5 850
Phenol ________
3e-2£r.e -- ______
Toluene - - _ - - - - - -
Ethyl Benzene ________
M.;r... lene Chloride 10 10 100 100 50 2,000 <5 500
PNAs
Naphthalene ________
Phenanthrene/Anthracene -- ______
Pyrene ________
Benzo(a)anthracene ________
Benzo(a)pyrene •______-_
AikvLbe-.zene (CgH^?) _____---
Alkylnapnthalene ^ci2Hi2^ ________
Phosphorus — - ___- _ —
Chlorine, wtS --------
Sulfur, we A - - - - - ~ ~ -
?C3s __-__--_
* Table A-2 identifies the source of analytical data for each used oil sample. Table A-3 provides
cod^s for each sample number which describe the specific generating source of used oil and the end-use.
A-3-
-------
TABLE A-l (continued)
ANALYTICAL DATA FOR USED OIL SAMPLES
Sample Number*
316
Flash Point (°F)
Metals
- Arsenic
Aluminum
Barium
Beryllium
Cadmium 1 . 3
Chromium 94
Cobalt
Copper 267
Iron 2,300
Lead 19
Magnesium
Manganese
Molybdenum
Nickel 31
Selenium
Silicon
Silver
Sodiun -
Tin 1.6
Titanium
Vanadium -
Zinc 543
Dichloroiiif luoromethane
Trichlorof luorome thane
Trichlorotr if luoroe thane
1 , 1 , 1-Trichloroe thane
Trichloroethylene
Te:rachloroechylene -
Phenol
Benzene -
Toluer.e
Etnyl Benzene
Xylenes
Me:'-."lene Chloride
317 318
125
_ _
20
30
-
0.3
1.0 10
- -
2.8 30
358 90
16 1,090
180
10
10
2.4 10
-
30
<10
130
<0.3 10
-
10
33 690
2
-
800
4
-
-
-
-
-
-
-
319
77
...
10
30
-
-
10
-
30
90
1,170
190
10
<10
<10
-
40
<10
120
10
-
10
720
500
-
400
650
-
_
-
-
-
.
-
2?o
72
—
10
20
-
-
10
-
30
60
920
110
10
<10
10
-
920
<10
110
10
-
10
750
150
-
60
2
-
-
-
-
-
_
-
321
85
_
10
30
_
_
10
_
30
90
1.170
190
10
<10
<10
_
40
<10
120
10
_
10
720
1
_
100
1
-
_
- -
-
.
_
_
322
135
" 10
10
_
_
40
«.
10
40
110
280
<10
<10
10
_
10
<10
50
10
_
40
130
10
_
200
5
-
_
-
_
_
_
_
^23
155
"<10
10
_
_
10
.
20
70
140
<10
<10
<10
10
_
10
<10
10
10
»
30
10
80
_
600
30
-
_
_
_
_
_
_
324
145
10
160
_
_
10
_
30
40
190
10
<10
<10
10
_
10
<10
30
10
_
10
550
150
_
4,100
50
-
—
_
.
_
_
_
PNAs
Naphthalene
Phenanthrene/ Anthracene
Pyrene
Benzo (a) anthracene
Ben?o(a)pyrene
Alkylbenzene
Alkylnaphthalene
Phosanarus
Chlorine, we 7.
Sulfur, wt %
PCBs
,,
(C ,H .,)
0.4
0.4
880
<50
880
<50
1,040
<50
880
<50
320
<50
180
<50
580
<50
* Table A-2 identifies the source of analytical data for each used oil sample. Table A-3 provides
codes for each sample number which describe the specific generating source of used oil and the end-use.
A-35
0251
-------
TABLE A-l (continued)
ANALYTICAL DATA FOR USED OIL SAMPLES
\
Sample Number*
325 126 327 128 329 330 131 * 332
Flash Point (°F) M ' "8 118 103 118
Metals _ _ - _
Arsenic ~ _
Aluminum ~~ _---~~
Barium ~~ ____--
Beryllium """___--
Cadmium ~~ ____--
Chromium ~ _
Cobalt "_"___--
Copper ~~ ____--
Iron ~ _ _ - — ~
Lead "_"__---
Magnesium ~" ___---
Manganese ~~ ___---
Molybdenum ""____--
Nickel ~ " ~_ • _
Selenium ""____--
Silicon ""____--
Silver ""___---
Sodium ~ _ - - -
Tin --"__---
Titanium ~~ ____--
Vanadium ~~ ___---
Zinc ~
Volatile Orgar.ics - 2 30 1 640 170
Dichlorodifluoromethane <10 J _____
Trichlorofluoromethane •- - ~ ~ _ _ _ _
TrichloTotrifluoroethane - - " " _60 40 2.200 3,100
1,1.1-Trichloroethane 180 130 »« ^ 3?o 5Q 73Q 490
Trichloroethylene 330 *u ^ 2Q 83Q 1>400
Tecrachloroethylene 60 ^ »u ^ _ _ _ _ •
Phenol ~~ ___---
Benzene ~ ~ _ __
Toluene ~ " ____--
Ethyl Benzene ~~" ___--
Xylenes ""___---
Methylene Chloride _
PtJAs ___---
Naphthalene ~ " ____--
Phenanthrene/Anthracene -'""___-
Pyrene ""___---
Benro(a)anthracene -""___--
Benzo(a)pyrene ~~~
Alkylbenzene
Alkylnaphthalene --'""
Phosphorus ""___---
Chlorine, wt2 ~~ __---
Sulfur, wt Z -<5Q -<5Q '<50 <50 <50 <50 <50 <50
PCBs
A-36
-------
TABLE A-l (continued)
ANALYTICAL DATA FOR USED OIL SAMPLES
Sample Number*!
334 335 336 337 338 339 340 341 342
Flash Point (°F) _________
Metals
Arsenic - - - - ~ ~ _ ^ - -
Aluminum _________
Barium _________
Beryllium _________
Cadmium - <1 <1 <1 <1 <1 <1 <1
-------
TABLE A-l (continued)
ANALYTICAL DATA FOR USED OIL SAMPLES
Sample Kuabers**
343 344 345 346 347 348 349 150
Flash Point (°F) - - - - - - _., _
Metals
Arsenic ________
Aluminum ________
Barium ________
Beryllium ________
Cadmium <1 <1 <1 <1 <1
-------
TABLE A-l (continued)
ANALYTICAL DATA FOR USED OIL SAMPLES
Sample Number*t
Flash Point (°F) ---------
Metals
Arsenic ------__
Aluainun ------_,"_,
Barium ---------
Beryllium ---------
Cadmium <1 <1 1 2 1 2 <1 <1 <1
Chromium 4 1 30 66 72 62 10 10 8
Cobalt ---------
Copper 86 1 200 540 48 52 23 42 40
Iron 275 30 3,100 1,600 250 440 220 1,160 220
Lead 230 5 62 230 300 260 350 40 430
Magnesium _________
Manganese - — ---,_- __
Molybdenum _---.__ _ _
Nickel <5 <5 38 8 <5 <5 <5 10 <5
Selenium _______ __
Silicon -----____
Silver _________
Sodium ---______
Tin _________
Titanium ---------
Vanadium ---------
:.-. so: : 200 1,100 -eo 620 870 190 i.oc;
Volatile Organics
Dichlorodiiiuoroaethane ---_-_-__
Trichlorofluoromethane ---------
Trichlorotrifluoroethane ---------
1,1,1-Trichloroethane ---------
Trichloroethylene ------J__
Tetrachloroetnyiene ------___
Phenol _--______
Benzene -_-___J__
Toluene - - ~ - - - - j
Ethvl Benzene -_-______
Xylenes -_-_--j__
Methylene Chloride _-----___
PNAs
Naphthalene _----____
Phenanthrene/Anthracene - - - - - - - _._
Pyrene ---______
Benzo(a)anthracene -_-______
Benzo(a)pyrene - -.» - - - - - -
Alitylbenzene (CgH^,) ---------
Alkylnaphthalene (C..H.,) -
Phosphorus i^J-'_
Chlorine, wtX _--__-___
Sulfur, utX -_-_--___
PCBs <6 <6 86 <15 <15 <15 <15 <15 <15
* Table A-2 identifies the source of analytical data for each used oil sample. Table A-3 provides
codes for each sample number which describe the specific generating source of used oil and the end-use.
; Indicates that the given constituent was detected but not quantified.
A-39
0253
-------
TABLE A-l (continued)
ANALYTICAL DATA FOR USED OIL SAMPLES
Sample Number* t
361 362 363 36*. 365 366 367 368
Flash Point (°F) -------_
Hetals
Arsenic -----__
Aluminum ____--__
Barium ________
Beryllium _-__--__
Cadmium <10 <10 <5 <2 <10 <10 <10 <10
Chromium <10 <10 35 6 <10 <10 <10 <10
Cobalt ----__..
Copper 23 32 6 9 90 60 <10 <10
Iron - 5,500 20 -
Lead 440 <10 65 260 <10 310 30 10
Magnesium ________
Manganese ----____
Molybdenum ________
Nickel <10 <10 - <5 <10 <10 <10 10
Selenium '----____
Silicon ________
Silver - - - - - -_
Sodium
Tin ---.-___
Titanium ----____
Vanadium -----.__
Zinc 760 18 35 95 380 1,100 <10 <10
Volatile Organics
Dichlorodifluoromethane ________
Trichlorofluoromethane -_--____
Trichlorotrifluoroethane --_-____
1,1,1-Trichloroethane -- $-____
Trichloroethylene -_ j J _ - _ _
Tetrachloroethylene ________
Phenol - - 6.2 - 8.7 4.8
Benzene _____ J J _
Toluene - _ - J J - j j
Ethyl Benzene - _____
Methylene Chloride ________
PSAs
Naphthalene _--_-___
Phenanthrene/Anthracene ________
Pyrene ________
Benzo(a)anthracene ________
Benzo(a)pyrene ________
Alkylbenzene (CgHi-,) --______
Alkylnaphthalene tc.-H,,) ________
Phosphorus lzi-_
Chlorine, wtZ ---_____
Sulfur, wtX ________
PCBs <17 <17 37 <0.9 <6 <21 <6 <6
* Table A-2 identifies the source of analytical data for each used oil sample. Table A-3 provides codes
for each sample number which describes the specific generating source of used oil and the end-use.
+ Indicates that the given constituent vas detected but not quantified.
A-40
-------
TABLE A-l (continued)
ANALYTICAL DATA FOR USED OIL SAMPLES
Sample Number* t
11°. 371 ,372 373 374 375 376 377 378
Flash Point (°F) - - - - - - -'-
Metals
Asaenic ----_____
Aluminum _________
Barium __-__-___
Beryllium _________
Cadmium 2 <1 <1 <1 1 <5 <10 <10 «10
Chromium 14 13 8 4 22 <10 <10 <10 <10
Cobalc _________
Copper 30 26 22 8 200 20 20 22 20
Iron - 34,000 -
Lead 320 300 300 190 58 330 430 430 420
Magnesium - _ • _
Manganese _______ _ _
Molybdenum ___ — _-__-
Nickel <5 <5 <5 <5 12 <10 <10 <10 <10
Selenium _________
Silicon _________
Silver _______ - _
Sodium _________
Tin _______ _ _
Titanium _________
Vanadium _________
Zi-.- 890 660 760 77 180 870 220 710 550
Volatile Organics
Dichlcrodifluoromethane _________
Irichiorof 1'uoromethane __--_--__
Trichlorotrifluoroethane ---------
1,1,1-Trichloroethane tJJt-J---
Trichloroethylene _________
Tetrachloroethylene _________
Phenol _________
Benzene i$Jt-----
Toluene t t"t t
Ethyl Benzene ___----__
X-,-_r.-= } i t t
Methylene Chloride _______ __
PSAs
Naphthalene _______ __
Phenanthrene/Anthracene _________
Pyrene _________
, Benzo(a)anthracene _________
Benzo(a)pyrene - - - ~ - ~ ~ - -'
Alkylbenzene (C9Hi2) -__---- _ _
Alkylnaphthalene (C]iHl2^ _-__--- _ _
Phosphorus _________
Chlorine, wt2 _________
Sulfur, wt % _________
PCBs <15 <15 <15 <15 <15 46 <17 <17
-------
TABLE A-l (continued)
ANALYTICAL DATA FOR USED OIL SAMPLES
Sample Number*!
— 380 381 382 383 384 365 386
Flash Point (°F) -------_
Metals
Arsenic - - - - _ _ _"_
Aluminum - - - - - - - ' _
Barium --------
Beryllium ------__
Cadmium <1 <1 <1 <1 1
-------
TABLE A-l (continued)
ANALYTICAL DATA FOR USED OIL SAMPLES
Sample Number* t
387 388 369 390 391 192 383 394 395
Flash Point (°F) _________
Metals
Arsenic - - - - - - _.,_ _
Aluminum _________
Barium _________
Beryllium _________
Cadmium <10 <10 <10 <10 <10 <10 <10 <10
Chromium <10 <10 <10 <10 <10 <10 <10 <10
Cobalt _________
Copper 20 20 20 20 20 20 <10 27
Iron _---_____
Lead 400 350 350 350 350 380 40 320
Magnesium _________
Manganese _________
Molybdenum _________
Nickel <10 <10 <10 <10 <10 <10 <10 <10
Selenium _._ _ _ _ _ _ _
Silicon - - -'-
Silver _________
Sodium - - - - - - • -
Tin _________
Titanium _________
Vanadium _________
Zinc 1.000 1.900 980 1,700 920 950 280 670
Volatile Cr^ir.ics
Dichlorodifluoromethane _________
Trichlorofluoromethane _________
Trichlorotrifluoroethane _________
1,1,1-Trichloroethane _________
Trichloroethylene JJttt+t--
Tetrachloroethylene - - - - - - - _._
Phenol 110 110 110 48 50 50 15 210 230
Benzene } * t t t J J
Toluene *********
Etnyl Benzene - - - - - - - - - -
Xylenes *****-- * J
Me:--:=-e Chloride _______ It
PNAs
Naphthalene _________
Phenanthrene/Anthracene _________
Pyrene ----_____
Benzo(a)anthracene _________
Benzo(a)pyrene _________
Alkylbenzene (CgH^) - ' -
Alkylnaphthalene (Cj^H^) -__----_-
Phosphorus ---__-___
Chlorine, wtX _________
Sulfur, wt % _________
PCBs <6 <9 <6 <20 <6 <25 89 <6 <18
* Table A-2 identifies the source of analytical data for each used oil sample. Table A-3 provides codes
for each sample number which describes the specific generating source of used oil and the end-use.
i Indicates that the given constituent was detected but not quantified.
A-43
025!
-------
TABLE A-l (continued)
ANALYTICAL DATA FOR USED OIL SAMPLES
Sample Number* i
22i ill 22§. 399 400 401 4Q2 403
Flash Point (°F) ------__
Metals
Arsenic ------__
Aluminum ------__
Barium - - - --
Beryllium ------__
Cadmium <10 <10 <10 <10 <10 <10 <10 <10
Chromium <10 <10 <10 <10 <10 <10 <10 <10
Cobalt - - - - - - ._
Copper <10 <10 <10 16 13 30 30 30
Iron ------__
Lead 70 20 50 140 260 420 100 90
Magnesium ------__
Manganese -----___
Molybdenum ------__
Nickel <10 <10 <10 <10 <10 <10 <10 <10
Selenium ------_«
Silicon -----.__
Silver ------__
Socur. ------__
Tin -'----___
Titanium -----___
Vanadium ------__
Zinc 50 <10 30 240 20 -
Volatile Organics
Dichlorodifluoromethane ---_____
Trichlorofluoromethane -----___
Trichlorotrifluoroethane ------__
1,1,1-Trichloroethane - J - - J
Trichloroethylene -----tt$
Tetrachloroethylene ------__
Phenol 11 39 48 21 -
Benzene -----___
Toluene ---ttttt
Ethyl Benzene -----___
Xylenes t $ J J
Methylene Chloride --tJ-JJt
PNAs
Naphthalene ----____
Phenanthrene/Anthracene --_-_-__
Pyrene ________
Benzo(a)anthracene --_-____
Benzo(a)pyrene -___-___
Alkylbenzene (C9Hi2) -__--___
Alkylnaphthalene tc.jH.-) -__---__
Phosphorus -___-.__
Chlorine, utZ -___-___
Sulfur, wtX ________
PCBs <225 <15 <14 <11 <6 81 15 <30
* Table A-2 identifies the source of analytical data for each used oil sample. Table A-3 provides code
for each sample number which describes the specific generating source of used oil and the end-use.
i Indicates that the given constituent was detected but not quantified.
A-44
-------
TABLE A-l (continued)
ANALYTICAL DATA FOR USED OIL SAMPLES
Sample Number*
Flash Point (°F)
Metals
Arsenic
Aluminum
Barium
Beryllium
Cadmium
Chromium
Cobalt
Copper
Iron
Lead
Magnesium
Manganese
Molybdenum
Nickel
Selenium
Silicon
Silver
Sodium
Tin
Titanium
Vanadium
Zinc
Volatile Organics
Dichlorodifluoromethane
Trichlorofluoromethane
Trichlorotrifluoroethane
1,1,1-Trichloroethane
Trichloroethylene
Tetrachloroethylene
Phenol
Benzene
Toluene
Ethyl Benzene
Xylenes
Methylene Chloride
PNAs
Naphthalene
Phenanthrene/Anthracene
Pyrene
Benzo(a)anthracene
Benzo(a)pyrene
Alkylbenzene (CgH^)
Alkylnaphthalene (Ci7%2^
Phosphorus
Chlorine, wt Z
Sulfur, wt %
PCBs
405
156
406
174
407 408 409 li°
212 212 97 212
T t
10
15
100
40
50
30
20
411
212
0
0
412 413
284 250
0 0
T T
100 100
50
30
20
1,500
600 0
7,200 0
600 0
5,000 0
74 0
* Table A-2 identifies the source of analytical data for each used oil sample. Table A-3 provides codes
for each sample nur-.ber which describes the specific generating source of used oil and the end-use.
t "T" indicates a trace amount of the given constituent was measured.
A-45
0256
-------
TABLE A-l (continued)
ANALYTICAL DATA FOR USED OIL SAMPLES
Sample Number*
Flash Point CF)
Metals
Arsenic
Aluminum
Barium
Beryllium
Cadmius
Chromium
Cobalt
Copper
Iron
Lead
Maenesiurr
Manganese
Molybdenum
Nickel
Selenium
Silicon
Silver
Sodium
Tin
Titanium
Vanadium
Zinc
Volatile Organics
Dichlorodifluoromethane
Trichlorofluoromethane
Trichlorotrifluoroechane
1,1,1-Trichloroethane
Trichloroethylene
Tetrachloroethylene
Phenol
Benzene
Toluene
Ethyl Benzene
Kylenes
Methylene Chloride
PSAs
Naphthalene
Phenanthrene/Anthracene
Pyrene
Benzo(a)anthracene
Benzo(a)pyrene
Alkylbenzene (CgHj^)
Alkylnaphthalene (C.,H12)
Phosphorus
Chlorine, wt X
Sulfur, wt %
PCBs
414 415 416 417 418 419
212 212 110 170 200 130
.300
420
212
421 I
118
5 0
100 300 0
150 150
300 300
20
25
40
20
20
15
210
300
1,200
8,300
6,900
1.300
5,400
6,000
* Table A-2 identifies the source of analytical data for each used oil sample. Table A-3 provides codes
for each sample number which describes the specific generating source of used oil and the end-use.
T Indicates that the given constituent was detected but not quantified.
-------
TABLE A-l (continued)
ANALYTICAL DATA FOR USED OIL SAMPLES
Sample Number*
Flash Point (°F)
Metals
Arsenic
Aluminum
Barium
Beryllium
Cadmium
Chromium
Cobalt
Copper
Iron
Lead
Magnesiun
Manganeee
Molybdenum
Nickel
Selenium
Silicon
Silver
Sodium
Tin
Titanium
Vanadium
Zinc
423 424 425 426 427 428
169 174
0 0 0 0 T f T
0 5 10 10 5 5
429 130 431
122 133 100
25
25 25 25 100 100
100 100
75
Dichlorodifluorome thane
Trichlorof luorone thane
Trichlorotrifluoroe thane
1,1, 1-Trichloroethane
Trichloroethylene
Tetrachloroethylene
Phenol
Benzene
Toluene
Ethyl Benzene
Xylenes
Methylene Chloride
PNAs
Naphthalene
Phenanthrene /Anthracene
Pyrene
Benzo (a) anthracene
Benzo(a)pyrene
Alkylbenzene (CgH,,)
Alkylnaphthalene tC.-H.,)
Phosphorus
Chlorine, wt 2
Sulfur, wt 7.
PCBs
400
3,000
100
10,000 , 9,000
0.43 1.25
000
0.46 0.38 0.46
000
* Table A-2 identifies the source of analytical data for each used oil sample. Table A-3 provides codes
for each sample number which describes the specific generating source of used oil and the end-use.
T Indicates that the given constituent was detected but not quantified.
A-47
0257
-------
TABLE A-l (continued)
ANALYTICAL DATA FOR USED OIL SAMPLES
Sample Number*
.432 433 434 435 436 437 438 439
Flash Point (°F> --------
Metals
Arsenic --------
Aluminum --------
Barium --------
Beryllium - - --
Cadmium --------
Chromium ______ __
Cobalt --------
Copper ----____
Iron --------
Lead --------
Magnesium --------
Manganese -_-_____
Molybdenum --------
XiCKel --------
Selenium --------
Silicon
Silver ________
Sodium _-__-___
Tin -----___
Titanium _--_____
Vanadium --------
Zinc --------
Volatile Organics
Dichlorodifluoromethane --______
Trichlorofluoromethane 680 7,500 460 1,003 5,200 55 - 238
Trichlorotrifluoroethane TttttJ-J
1,1,1-Trichloroethane 3,100 1,334 6,300 491 4,631 1,500 1,100 1,300
Trichloroethylene 410 240 2,900 230 1,049 900 5,000 751
Tetrachloroethylene 700 100 106 65 302 540 14 163
Phenol --____ __
Benzene ______ __
Toluene ------ __
Ethyl Benzene --__-___
Xylenes ______ __
Methylene Chloride _-_-__ __
PNAs
Naphthalene ______ __
Phenanthrene/Anthracene ______ __
Pyrene _-__-___
Benzo(a)anthracene ___--_ __
Benzo(a)pyrene _._
Alkylbenzene (CgHj^) _-__-___
Alkylnaphthalene (C,2Hi2^ ------ -_
Phosphorus ______ __
Chlorine, wt% -__-__._
Sulfur, wtZ ________
PCBs 265 <40 <40 <40 <40 110 110 63
* Table A-2 identifies the source of analytical data for each used oil sample. Table A-3 provides code
for each sample number which describes the specific generating source of used oil and the end-use.
I Indicates that the given contaxinant was detected but not quantified.
A-48
-------
TABLE A-l (continued)
ANALYTICAL DATA FOR USED OIL SAMPLES
Sample Number*
442 443 444 445 446 447 448 449
flash Point (*F)
Metals
Arsenic
Aluminum
Barium
Beryllium
Cadmium
Chromium
Cobalt
Copper
Iron
Lead
Magnesium
Manganese
Molybdenum
Nickel
Selenium
Silicon
Silver
Sodium
Tin
Titanium
Vanadium
Volatile Organics
Dichlorodifluoromethane _________
Trichlorofluoromethane 280 ___ 3 24 - - -
Trichlorotrifluoroethane ttttttt--
1,1,1-Trichloroethane 340 83 2,500 760 980 810 31 240 240
Trichloroethylene 1,000 36 670 520 410 360 36 15
Tetrachloroethylene 140 11 480 200 120 96 320 7
Phenol - _ - - . -
Benzene - ________
Toluene - -"-
Ethyl Benzene - ________
Xylenes _________
Methylene Chloride - - - - - -
PSAs
Naphthalene _________
Phenanthrene/Anthracene _________
Pyrene . _________
Benzo(a)anthracene _________
Benzo(a)pyrene _________
Alkylbenzene (C^H,,) --_----__
Alkylnaphthalene tt^H^) -____-___
Phosphorus _________
Chlorine, wt % _________
Sulfur, wtZ _________
PCBs <40 <40 <40 <40 66 <40 240 <40 <-0
* Table A-2 identifies the source of analytical data for each used oil sample. Table A-3 provides codes
for eacn sample number which describes the specific generating source of used oil and the end-use.
I Indicates that the given contaminant was detected but not quantified.
A-49
0258
-------
TABLE A-l (continued)
ANALYTICAL DATA FOR USED OIL SAMPLES
Saaple Number*
450 451 452 453 454 455 456 457
Flash Point (*F) ________
Metals
Arsenic - - - - - - -"_
Aluminum ________
Barium ________
Beryllium ________
Cadmium ________
Chromium -- ______
Cobalt ________
Copper ________
Iron ________
Lead ________
Magnesium ________
Manganese ________
Molybdenum ________
Nickel ________
Selenium ________
Silicon - - - - - -'-
Silver ________
Sodium ________
Tin ________
Titanium ________
Vanadium ________
Volatile Organics
Dichlorodifluoromethane ________
Trichlorofluoromethane ________
Trichlorotrifluoroethane -$$__--_
1,1,1-Trichloroethane - 1,100 83 270 2 18 3 1,200
Trichloroethylene - 19 60 128 - _ _ u
Tetrachloroethylene " 77 2,000 22 110 - 7 430
Phenol _________
Benzene -'-
Toluene - - • -
Ethyl Benzene ________
Xylenes ________
Methylene Chloride -- ______
PNAs
Naphthalene ________
Phenanthrene/Anthracene - - - - _•-•_
.Pyrene ________
Benzo(a)anthracene -- ______
Benzo(a)pyrene -- ______
Alkylbenzene (CqH,,)
Alkylnaphthalene tc1
Phosphorus
Chlorine, wtZ ________
Sulfur, ut/i ________
PCBs <40 <40 <40 170 <40 38 <40 <40
* Table A-2 identifies the source of analytical data for each used oil sample. Table A-3 provides codes
for each sample number which describes the specific generating source of used oil and the end-use,
i Indicates that the given contaminant was detected but not quantified.
A-50
-------
TABLE A-l (continued)
ANALYTICAL DATA FOR USED OIL SAMPLES
Sample Number*
459
Flash Point (°F)
Metals
Arsenic
Aluminum
Barium
Beryllium
Cadmium
Chromium
Cobalt
Copper
Iron
Lead
Magnesium
Manganese
Molybdenum
Nickel
Selenium
Silicon
Silver -
Sodium
Tin
Titanium
2inc
Volatile Organics
Dichlorodifluoronethane
Trichlorofluoromethane 690
Trichlorotrifluoroethane J
1,1,1-Trichloroethane 730
Trichloroethylene 18
Tetrachloroethylene 100
Pher.ol
Benzene
Toluer.e
Etr.yl Benzene
Xylenes
Methylene Chloride
PNAs
Naphthalene
Phenanthrene/Anthracene
Pyrene
Benzo(a)anthracene
Benzo(a)pyrene
Alkylbenzene (C-H,.)
Alkylnaphthalene tt,,H.,)
Phosphorus "
Cr.lcrine, wt %
Sulfur, WE %
PCBs 44
* Table A-2 identifies the source of analytical data for each used oil sample. Table A-3 provides codes
for each sample number which describes the specific generating source of used oil and the end-use.
I Indicates that the given constituent was detected but not quantified.
A-51
0250
-------
TABLE A-l (continued)
ANALYTICAL DATA FOR USED OIL SAMPLES
Sample Number *
<32
<0.32
1.6
2.9
37
<0.29
1.1
3.0
48
<0.36
<0.36
3.4
101
<0.34
1.3
3.8
<39
<0.39
0.55
<0.8
25
<0.25
1.4
364
<35
<0.35
<0.35
<0.7
<36
<0.36
<0-36
<0.7
460 461 £62 463 464 465 466 467
Flash Point (°F) - - - - - - _'"_
Metals
Arsenic ______ __
Aluminum ---__-__
Barium
Beryllium
Cadmium
Chromium
Cobalt
Copper --------
Iron - - - - _ _._
Lead 380 670 390 790 <1.94 1,900 <1.9 4.7
Magnesium - - - - . - . _ _
Manganese ------__
Molybdenum -----___
Nickel 2.0 <1.4 3.3 5.0 6.6 <1.3 2.1 <1.8
Selenium ----__ __
Silicon ------,_
Silver ------__
Sodium ---.__ _ _
Tin -----.___
Vanadium --_-._ __
Zinc ----_-__
Volatile Organics
Dichlorodifluoromethane ----____
Trichlorofluoromethane ---_-___
Trichlorotrifluoroethane --__-___
1,1,1-Trichloroethane ----____
Trichloroethylene -----___
Tetrachloroethylene -----___
Phenol --______
Benzene -----___
Toluene -_---___
Ethyl Benzene - - - _ . -
Xylenes --_-.___
Methylene Chloride -----___
PNAs
Naphthalene -_---___
Phenanthrene/Anthracene _----___
Pyrene -----___
Benzo(a)anthracene ----____
Benzo(a)pyrene -_--____
Alkylbenzene (CgHjO ---_-___
Alkylnaphthalene tc12H12) ---_-___
Phosphorus --______
Chlorine 260 370 1,330 1,380 459,000 6,150 40 55
Sulfur, vt Z 0.32 0.39 0.35 0.38 0.10 0.46 0.33 0.34
PCBs <3 <3 <3 135 <3 <3 <3 <3
* Table A-2 identifies the source of analytical data for each used oil sample. Table A-3 provides cod
for each sample number which describes the specific generating source of used oil and the end-use.
A-5:
-------
TABLE A-l (continued)
ANALYTICAL DATA FOR USED OIL SAMPLES
Sample Number *
<38
<0.38
1.0
4.7
96
<0.31
0.92
4.4
<49
<0.049
<0.49
<1
<43
<0.43
1.8
6.2
147
<0.26
1.1
29
<29
<0.29
6.3
16
<34
<0.35
1.0
5.4
<32
<0.32
<0.32
1.2
<29
<0.30
9.6
16
469 ±22. il1. ±72. 473 474 475 476 477
Flash Point (*F) - - - _ _ _ _'_
Metals
Arsenic _________
Aluminum ----_____
Barium
Beryllium
Cadmium
Chromium
Cobalt
Copper -_-______
Iron -_--_-.___
Lead 1,700 370 120 590 810 16 18 4.8 31
Magnesium _______
Manganese -------T-
Molybdenun -_--_-___
Nickel 1.9 2.4 22 2.3 3.9 52 7.9 <1.6 90
Selenium _________
Silicon _________
Silver -----____
Sodium ------___
Tin -_-______
Vanadium __»______
Zinc ---__-___
Volatile Organics
Dichlorodifluoromethane ---______
Tnchlorof luoromethane _________
Trichlorotrifluoroethane __--_____
1,1,1-Trichloroethane -_----_.__
Trichloroethylene ------___
Tetrachioroechyiene _--__-___
Phenol - -"-
Ber.zene ------___
Toluene __--_-___
Ethyl Benzene _--__-___
Xylenes _-----___
Methylene Chloride -_----___
PNAs
Naphthalene -_--_-___
Phenanthrene/Anthracene _--_--___
Pyrene - _.----___
Ber.zo (a) anthracene -_--_____
Benzo(a)pyrene _-__--___
Alkylbenzene (C9H,2) --_---___
Alkylnaphthalene (C.-Hj^.) _________
Phosphorus _________
Chlorine 640 1,410 660 1.390 2,370 3,000 14,000 6,G 19,800
Sulfur, vi" 0.83 0.26 1.35 0.49 1.30 0.50 <0.10 0.02 <0.6
PCBs <3 81 <3 <3 <3 <3 529 <3 <3
0260
si dara for each used oil sar.ole. Table A-3 provides codes
-------
TABLE A-l (continued)
ANALYTICAL DATA FOR USED OIL SAMPLES
Sample Number *
121 ___> <.80 481 482 483 484 485
Flash Point (°T) - - - - 154 165 168 134
Metals
Arsenic - <2 10.6 - 2.9
Aluminum _ _ _ _____
Barium <35 <23 <45 <38
Beryllium <0.35 <0.23 <0.45 <0.38 -
Cadmium 0.78 3.8 <0.45 <0.38 1.2 <1 <1 :
Chromium 0.84 7.0 1.1 7.7 4.2 8.4 - 9.6 (
Cpbalt ________
Copper _-__-___
Iron _-__-___
Lead 6.3 25 4.9 380 -
Magnesium ________
Manganese ________
Molybdenum ________
Nickel 5.6 ________
Phosphorus ______ _ -
Chlorine 302 72,500 1,360 610 2,170 747 - 1,300
Sulfur, wt % 0,78 <0.10 0.57 0.31 0.55 0.45 0.55 0.42
PCBs <3 <3 <3 24.1 <3 <3 <3 <3
* Table A-2 identifies the source of analytical data for each used oil sample. Table A-3 provides codes
for each sample number which describes the specific generating source of used oil and the end-use.
-------
TABLE A-l (continued)
ANALYTICAL DATA FOR USED OIL SAMPLES
Sample Number
487 486 489 A90
Flash Point (*F) 126 120 130 128
Metals
Arsenic -
Aluminum - - -
Barium -
Beryllium -
Cadmium - - - <1
Chromium - - - 11.0
Cobalt -
Copper -
Iron -
Lead -
Magnesium -
Manganese -
Molybdenum - - - ,
Nickel - - - 8.8
Selenium - - - 2.6
Silicon -
Silver -
Sodium - - - -
Tin -
Titanium -
Var.sci-- -
Zinc -
Volatile Organics
Dichlorodifluoromethane -
Trichlorofluoromethane -
Trichlorotrifluoroethane -
1,1,1-Tnchloroethane -
Trichloroethylene -
Tetrachloroethylene -
Pneno- -
Benzene - i-
Toluene -
Ethyl Benzene -
Xylenes - - - -
Methylene Chloride _
PNAs
Naphthalene -
Phenanthrene/Anthracene -
Pyrene -
Benzo(a)anthracene -
Benzo(a)pyrene - - - _
Alkylbenzene
Alkylnaphthalene
Phosphorus -
Chlorine - 1,240
Sulfur, wt Z 0.59 0.63 0.60 0.56
PCBs <3 4.62 44.8 <3
* Table A-2 identifies the source of analytical data for each used oil sample. Table A-3 provides codes
for each sanple number which describes the specific generating source of used oil and the end-use.
A-55
0261
-------
TABLE A-l (continued)
ANALYTICAL DATA FOR USED OIL SAMPLES
Sample Number*
Flash Point (*F)
Metals
Aluminum
Arsenic
Barium
Beryllium
Cadmium
Chromium
Cobalt
Copper
Iron
Lead
Magnesium
Manganese
Molybdenum
Nickel
Selenium
Silicon
Silver
Sodium
Tin
Titanium
491
>147
-
<5
490
-
<10
-
-
51
753
477
"
"
<5
8
<5
-
<8
-
-
-
492
>147
-
<5
320
-
<10
-
-
59
654
592
-
—
7
<5
<5
-
<8
-
-
-
493
>147
-
<5
1,160
—
<10
—
—
17
11
<5
—
—
<5
<5
<5
-
<8
-
-
-
494
>147
—
<5
730
—
<10
— •
—
103
1,030
538
—
—
<5
12
<5
-
<8
-
-
—
495
>147
-
<5
550
—
<10
—
-
85
826
484
••
"
<5
9
<5
-
<8
-
-
-
496
>147
-
<5
630
-
<10
-
-
96
731
631
-
—
5
8
<5
-
<8
-
-
-
497
>147
-
<5
110
—
<10
-
—
9
114
<5
-
-
<5
<5
<5
-
<8
-
-
-
498
>JL47
—
<5
1.710
—
<10
-
—
89
978
<5
—
—
<5
15
<5
-
<8
-
-
—
Zinc
Volatile Organics
Dichlorodifluoromethane
Trichlorofluoromethane
Trichlorotrifluoroethane
1,1,1-Trichloroethane
Trichloroethylene
Tetrachloroethylene
Phenol
Benzene
Toluene
Ethyl Benzene
Xylenes
Methylene Chloride
PNAs
Naphthalene
Penanthrene/Anthracene
Pyrene
Benz o(a)an thracene
Benzo(a)pyrene
15 6 <5 10 8 S <5 10
933 1,060 1,090 1,760 1.590 1.860 1,300 2.050
1.400 <200
<200 <200
610 <200
<200
<200
<200
<200
<200
<200
<200
<200
700
<200
<200
<200
<200
<200
<200
Alkylbenzene
Alkylnaphthalene
Phosphorus
Chlorine, wt Z
Sulfur, wt Z
PCBs
0.40 0.19
0.60 0.49
<30 <30
0.03
0.83
0.33
0.63
<30
0.47
0.68
<30
0.42
0.64
<30
0.42
1.01
<30
0.43
0.62
* Table A-2 identifies the source of analytical data for each used oil sample. Table A-3 provides codes
for each sample number which describes the specific generating source of used oil and the end-use.
A-56
-------
TABLE A-l (continued)
ANALYTICAL DATA FOR USED OIL SAMPLES
Sample Number*
Flash Point (°F)
Metals
Aluminum
Arsenic
Barium
Beryllium
Cadmium
Chromium
Cobalt
Copper
Iron
Lead
Magnesium
Mar.ganese
Molvbdenum
Nickel
Selenium
Silicon
Silver
Sodium
Tin
Titanium
Vanadium
Zinc
499
-
-
<5
310
-
<10
-
—
245
6,360
1,320
—
-
14
133
<5
-
<8
-
-
-
90
1,860
500
-
-
36
70
-
<10
-
-
30
245
<5
—
—
<5
11
<5
-
12
-
-
-
7
192
501
-
-
<5
1.170
-
<10
-
-
898
34,100
4,730
—
-
84
793
<5
-
15
-
-
-
245
3,800
502
>147
-
<5
750
-
<10
-
—
59
950
201
~
—
<5
6
<5
-
<5
-
-
-
22
495
503
>147
-
<5
460
-
<10
-
-
61
402
958
—
—
6
<5
<5
-
<5
-
-
-
11
1,190
504
>147
-
<5
160
-
<10
-
-
101
1,590
1.180
•
-
<5
<5
<5
-
<5
-
-
-
8
1,130
Volatile Orgar.izs
Dichlorodifluoromethane
Trichlorofluoromethane
Trichlorotrifluoroethane
1,1,1-Trichloroethane
Trichloroethylene
Tetrachloroethylene
Phenol
Benzene
Toluene
Ethyl Benzene
Xylenes
Methvlene Chloride
<200
<200
<200
210 720
<200 <200
360 <200
PNAs
Naphthalene
Penanthrene/Anthracene
Pyrene
Benzo(a)anthracene
Benzo(a)pyrene
Alkylbenzene (CgH
Alkylnaphthalene
Phosphorus
Chlorine, wt %
Sulfur, wt 7.
PCBs
0.25 0.18
0.26 0.16
0.20 .0.24 0.16 0.22
0.25 0.44 0.51 0.30
<50 <10 <10
* Table A-2 identifies the source of analytical data for each used oil sample. Table A-3 provides codes
for each sample number which describes the specific generating source of used oil and the end-use.
A-57
0262
-------
TABLE A-l (continued)
ANALYTICAL DATA FOR USED OIL SAMPLES
Sample Number*
Flash Point (°F)
Metals
Aluminum
Arsenic
Barium
Beryllium
Cadmium
Chromium
Cobalt
Copper
Iron
Lead
Magnesium
Manganese
Molybdenum
Nickel
Selenium
Silicon
Silver
Sodium
Tin
Titaniur.
Vanadium
Zinc
Volatile Organics
Dichlorodif luorome thane
Trichlorof luorome thane
Trichlorotr if luoroe thane
1,1, 1-Tr ichloroethane
Trichloroecr.ylene
Tetrachloroethylene
Phenol
Benzene
Toluene
Ethyl Benzene
Xylenes
Methylene Chloride
505
>147
-
<5
60
-
<10
-
-
49
173
926
-
-
<5
<5
<5
-
«8
-
-
-
12
669
-
-
-
1,800
540
<200
-
-
-
-
-
-
506
>U7
-
<5
140
-
<10
-
-
263
5,350
484
-
-
<5
37
<5
-
<8
-
-
-
26
688
-
-
-
-
-
-
-
-
-
-
-
-
507
>147
-
<5
130
-
<10
-
—
137
4,220
932
-
-
7
26
<5
-
<8
-
-
-
26
1,520
-
-
-
<200
<200
<200
-
-
-
-
-
-
508
>147
.
<5
100
-
<10
-
-
46
1,690
786
-
-
<5
10
<5
-
<8
-
-
-
26
807
-
-
-
<200
1,200
<200
-
-
-
-
-
-
509
>H7
-
<5
<50
-
<10
-
-
<5
15
55
-
-
<5
<5
<5
-
<8
-
-
-
<5
49
-
-
-
610
<200
<200
-
-
-
-
-
-
510
^™*^~ »*
>147
_
<5
70
-
<10
-
_
57
551
918
-
-
<5
<5
<5
-
<8
-
-
-
9
941
—
-
_
<200
<200
<200
—
-
-
-
-
-
PNAs
Naphthalene
Penanthrene/Anthracene
Pyrene
Benzo(a)anthracene
Benzo(a)pyrene
Alkylbenzene (C_H--)
Alkylnaphthalene 1C. ,IL,)
Phosphorus l
Chlorine, wt X
Sulfur, wt Z
PCBs
0.32
0.40
<20
0.19
0.22
0.17
0.25
<50
0.64
0.52
<100
0.11
0.09
<20
0.11
0.36
<20
* Table A-2 identifies the source of analytical data for each used oil sample. Table A-3 provides codes
for each sample number which describes the specific generating source of used oil and the end-use.
A-58
-------
TABLE A-l (continued)
ANALYTICAL DATA FOR USED OIL SAMPLES
Sample Number*
511 512
Flash Paint (8F) >147 >147
Metals
Aluminum
Arsenic <5 <5
Barium 400 70
Beryllium
Cadmium <10 <10
Chromium - ~
Cobalt
Copper 199 14
Iron 823 28
Lead 389 165
Magnesium
Manganese ~
Molybdenum 11 <5
Nickel 6 <5
Selenium <5 <5
Silicon
Silver <5 <8
Sodium
Tin
Titanium
Vanadium 9 <5
Zinc 741 51
.'cl_-.lie Crgar.-cs
Dichlorodifluoromethane
Trichlorofluoromethane
Trichlorotrifluoroethane
1.1.1-Trichloroetluuie 530 280
Trichloroethylene <200 <200
Tetrachloroethylene "250 <200
Phenol
Benzene
Toluene -
ttn\i Benzene -
Xylenes
Methvlene Chloride
PNAs
Naphthalene
Penanthrene/Anthracene
Pyrene
. Benzo(a)anthracene
Benzo(a)pyrene
Alkylbenzene (CgH
Alkylnaphthalene
Phosphorus
Chlorine, wt % 0.22 0.08
Sulfur, wt % 0.29 0.39
PCSs <20 <10
* Table A-2 identifies the source of analytical data for each used oil sample, table A-3 provides codes
for each sample number which describes the specific generating source of used oil and the end-use.
A-59
0263
-------
ANALYTICAL DATA FOR USED OIL SAMPLES
Flash Point (°F)
Metals
Aluminum
Arsenic
Barium
Beryllium
Cadmium
Chromium
Cobalt
Copper
Iron
Lead
Magnesium
Manganese
Molybdenum
Nickel
Selenium
Silicon
Silver
Sodium
Tin
Titanium
Vanadium
Zinc
Volatile Organics
Dichlorodifluorome thane
Trichlorof luorome thane
1,1, 1-Tr ichloroethane
Trichloroethylene
Tetrachloroethylene
Phenol
Benzene
Toluene
Ethyl Benzene
Xylenes
Methylene Chloride
513
>147
-
<5
200
-
<10
-
-
102
460
1,630
-
-
7
<5
<5
-
<9
-
-
-
<5
2,060
-
—
220
<200
<200
-
-
-
-
-
-
514
>147
-
<5
90
-
<10
-
-
44
155
635
-
-
5
<5
<5
-
<9.
-
-
-
<5
449
-
—
460
<200
300
-
-
-
-
-
-
515
>147
-
<5
120
-
<10
-
-
109
6,110
443
-
-
10
11
<5
-
<9
-
-
-
34
422
-
—
540
<200
340
-
-
-
-
-
-
Sample t
516
>147
-
<5
160
-
<10
-
-
61
412
1,110
-
-
<5
<5
<5
-
<9
-
-
-
<5
1,080
-
-
2,200
340
<200
-
-
-
-
-
-
147
.
<5
210
-
<10
-
_
59
404
1.790
-
-
6
<5
<5
-
<9
-
-
.
<5
1,250
-
-
<200
<200
<200
-
-
-
-
-
-
518
>147
_
<5
<50
-
<10
-
_
22
90
107
-
-
<5
<5
<5
-
<9
-
-
-
<5
727
-
-
<200
<200
<200
-
-
-
-
-
-
519
>147
_
<5
100
-
_
•
40
224
1,740
-
-
7
<5
<5
_
<9
-
-
-
<5
1,470
-
-
<200
<200
<200
-
-
-
-
-
-
520
>147
_
<5
140
• -
9
_
_
71
441
774
-
-
15
6
<5
-
<5
-
-
_
13
699
-
-
620
110
1,800
—
-
-
-
-
-
PN'As
Naphthalene
Penanthrene/Anthracene
Pyrene
Benzo(a)anthracene
Benzo(a)pyrene
Alkylbenzene (C,R,2)
Alkylnaphthalene tc,2H13)
Phosphorus
Chlorine, wt %
Sulfur, wt Z
PCBs
0.06
0.33
0.08
0.25
0.23
0.25
0.24
0.34
0.15
0.33
0.04
0.52
0.13
0.29
0.21
0.28
* Table A-2 identifies the source of analytical data for each used oil sample. Table A-3 provides codes
for each sample number which describes the specific generating source of used oil and the end-use.
A-60
-------
TABLE A-l (continued)
ANALYTICAL DATA FOR USED OIL SAMPLES
Sample Number*
Flash Point (°F)
Metals
Aluminum
Arsenic
Barium
Beryllium
Cadmium
Chromium
Cobalt
Copper
Iron
Lead
Magnesium
Manganese
Molybdenum
Nickel
Selenium
Silicon
Silver
Sodium
Tin
Titar.iuc
Vanadium
Zinc
Vclazi.e ^rgar.ics
Dichlorodif luorome thane
Trichlorof luorome thane
Trichlorotrifluoroe thane
1,1, 1-Tr ichloroethane
trichloroethylene
Te trachloroe thy lene
Phenol
Benzene
Toluene
Ethyl Benzene
Xylenes
Methylene Chloride
521
>147
-
<5
160
-
<7
-
-
56
433
942
-
-
6
12
<5
-
<5
-
-
-
20
678
-
-
-
1,700
230
1,000
-
-
-
- .
-
-
522
>147
-
<5
160
-
<7
-
-
93
1.020
543
-
-
9
12
<5
-
<5
-
-
-
23
628
-
-
-
<100
<100
460
-
-
-
-
-
-
523
>147
-
<5
90
-
<7
-
-
73
467
917
-
-
<5
7
<5
-
<5
-
-
-
7
872
-
-
-
2.000
180
300
-
-
-
-
-
-
524
>147
-
<5
140
-
<7
-
—
42
301
602
-
-
<5
8
<5
-
<5
-
-
-
12
562
-
-
-
1.200
770
2,500
-
-
-
-
-
-
525
>147
_
<5
60
-
<7
-
-
37
792
68
-
-
<5
11
<5
-
<5
-
-
-
36
156
-
-
-
220
<100
<100
-
-
-
-
-
-
526
>147
_
<5
<50
-
<7
-
_
84
616
48
-
-
5
10
<5
-
<5
-
-
-
11
97
-
-
-
1.400
490
<100
-
-
-
-
-
-
527
>147
_
<5
<60
-
<7
-
-
46
470
361
-
-
9
11
<5
-
<5
-
-
-
7
451
-
-
-
400
180
200
-
-
-
-
-
-
528
>147
> —
<5
<90
-
<7
-
_
56
265
935
-
-
5
<5
<5
-
<5
-
-
-
<5
857
-
-
-
1.400
120
170
-
-
-
-
-
-
PSAS
Naphthalene
Penanthrene /Anthracene
Pyrene
Benzo (a) anthracene
Benzo(a)pyrene
Alkylbenzene (C.H )
Alkylnaphthalene
Phosphorus
Chlorine, wt %
Sulfur, wt '/.
PCBs
0.42
0.49
<5
0.13
0.24
<5
0.22
0.31
<5
0.92
0.64
<5
0.32
0.80
<10
0.28
0.41
<5
0.19
0.47
<5
0.24
0.47
<5
* Table A-2 identifies the source of analytical data for each used oil sample. Table A-3 provides codes
for each sample number which describes the specific generating source of used oil and the end-use.
A-61
0264
-------
TABLE A-l (continued)
ANALYTICAL DATA FOR USED OIL SAMPLES
Flash Point ("F)
Metals
Aluminum
Arsenic
Barium
Beryllium
Cadmium
Chromium
Cobalt
Copper
Iron
Lead
Magnesium
Manganese
Molybdenum
Nickel
Selenium
Silicon
Silver
Sodium
Tin
Titanium
Vanadium
Zinc
529
>147
-
<5
100
-
<7
-
-
80
986
551
-
-
7
13
<5
-
7
-
-
-
16
655
530
>147
-
<5
180
-
<7
_
_
56
932
239
-
-
13
9
<5
-
<5
-
-
-
19
206
531
>147
-
<5
210
-
<7
_
_
ISA
1,720
728
-
-
23
18
<5
-
<5
-
-
-
27
862
Sample
532
>147
-
<5
220
-
<7
_
_
167
1,090
757
-
-
30
14
<5
-
8
-
-
-
20
720
Number*
533
>147
-
<5
240
-
<7
_
_
147
1,100
717
-
-
11
17
<5
-
<5
-
-
-
65
825
534
>147
_
<5
220
_
<7
.,
»
96
1,410
343
-
-.
18
11
<5
-
<5
-
-
-
39
310
535
>147
_
<5
170
_
<7
_.
.
95
6,650
386
-
_
17
16
<5
-
<5
-
-
-
56
906
536
>U7
_
<5
190
_
<7
_
_
180
2,110
1.570
-
_
61
13
<5
-
<5
-
-
-
36
662
Volatile Organics "
Dichlorodifluoromethane
Trichlorofluoromethane
Trichlorotrifluoroethane
1,1,1-Trichloroethane
Trichloroethylene
Tetrachloroethylene
Phenol
Benzene
Toluene
Ethyl Benzene
Xylenes
Methylene Chloride
1,300 1,100
<100 160
560 880
740
<100
840
970
<100
4,200
2,000
120
140
2.500
320
700
<100 3,100
<100 <100
<100 8.800
PNAs
Naphthalene
Penanthrene/Anthracene
Pyrene
Benzo(a)anthracene
Benzo(a)pyrene
Alkylbenzene (C.R,-)
Alkylnaphthalene tc.-tt,,)
Phosphorus
Chlorine, vt Z
Sulfur, vt Z
PCBs
0.
0.
17
28
<2
0.
0.
<
25
51
10
0.17
0.36
<5
0.32
0.36
<5
0
0
.26
.66
56
0
0
.20
.46
24
0.04 0.95
0.40 0.36
<1 <2
* Table A-2 identifies the source of analytical data for each used oil sample. Table A-3 provides codes
for each sample number which describes the specific generating source of used oil and the end-use.
A-62
-------
TABLE A-l (continued)
ANALYTICAL DATA FOR USED OIL SAMPLES
Sample Number*
Flash Point (°F)
Metals
Aluminum
Arsenic
Barium
Beryllium
Cadmium
Chromium
Cobalt
Copper
Iron
Lead
Magnesium
Manganese
Molybdenum
Nickel
Selenium
Silicon
Silver
Sodium
Tin
Titanium
Vanadium
Zinc
Volatile Organics
Dichlorod if luorome thane
Trie hlorof luorome thane
Trichlorotrif luoroethane
1 ,1 , 1-Trichloroethane
Trichloroethylene
Tetrachloroethylene
Phenol
Benzene
Toluene
Ethyl Benzene
Xylenes
Methylene Chloride
537
>147
-
<5
160
-
<7
-
-
74
739
753
-
-
8
8
<5
-
<5
-
-
-
41
966
-
-
-
15 ,000
<100
1,300
-
-
-
-
-
-
538
140
-
<5
110
-
<7
-
-
63
803
821
-
-
6
14
<5
-
<5
-
-
-
64
677
-
-
-
470
<100
<100
-
-
-
-
-
-
539
>147
-
<5
160
-
<7
-
-
83
870
558
-
—
<5
14
<5
-
<5
-
-
-
28
640
-
-
-
3,400
190
2,400
-
-
-
-
-
-
540
90
-
<5
160
-
<7
-
-
89
1,160
564
-
—
6
10
<5
-
<5
-
-
-
24
789
—
-
-
3,200
330
3,100
-
-
-
-
™-
-
541
>147
-
<5
270
-
<7
-
-
217
815
1,080
-
—
49
17
<5
-
<5
-
-
-
36
664
—
-
-
1,200
110
6,400
—
-
—
—
~
-
542
>147
-
<5
130
-
<7
-
-
91
915
693
-
-
8
11
<5
-
<5
-
-
-
46
830
-
-
-
1,400
<100
610
-
-
-
-
—
-
543
>147
-
<5
190
-
<7
-
-
169
2,320
957
-
-
36
15
<5
-
<5
-
-
-
29
905
—
-
-
4.500
280
8,800
—
-
-
—
—
—
544
126
-
<5
140
-
<7
-
-
89
314
640
-
-
12
7
<5
-
<5
-
-
-
45
604
—
-
-
420
120
3,800
—
-
—
—
~
—
PNAs
Naphthalene
Penanthrene/Anthracene
Pyrene
Benzo(a)anthracene
Benzo(a)pyrene
Alkylbenzene (CgH,.)
Alkylnaphthalene tc^H^)
Phosphorus
Chlorine, vt Z
Sulfur, wt %
PCBs
-
—
0.77
0.43
<5
-
—
0.13
0.37
<5
—
~
0.28
0.35
<5
•
*
0.26
0.33
<5
-
•"
0.42
0.37
<5
-
~
0.21
0.40
<5
—
~
0.58
0.36
<5
-
••
0.29
0.39
<5
* Table A-2 identifies the source of analytical data for each used oil sample. Table A-3 provides codes
for each sample number which describes the specific generating source of used oil and the end-use.
A-63
0261
-------
TABLE A-l (continued)
ANALYTICAL DATA FOR USED OIL SAMPLES
Sample Number*
Flash Point (*F)
Metals
Aluminum
Arsenic
Barium
Beryllium
Cadmium
Chromium
Cobalt
Copper
Iron
Lead
Magnesium
Manganese
Molvbdenum
Nickel
Selenium
Silicon
Silver
Sodium
Tin
Titanium
Vanaoiur
Zinc
Volatile -Organics
Die hlorodifluorome thane
Trichlorofluoromethane
Trichlorotrifluoroe thane
1,1, 1-Trichloroethane
Tr ichloroe thy lene
Tetrachloroethylene
Phenol
Benzene
Toluene
Ethyl Benzene
Xylenes
Methylene Chloride
545
>147
-
<5
140
-
<7
-
_
112
1,170
1,170
-
-
<5
14
<5
-
<5
-
-
-
10
1,090
-
-
-
3,300
620
830
- ,
-
-
-
-
—
546
>147
-
<5
160
-
<7
-
-
48
450
927
-
-
<5
8
<5
-
<5
-
-
-
10
622
-
-
-
3,000
540
760
-
-
-
-
-
—
547
>147
-
<5
150
-
<7
-
-
55
458
867
-
-
7
8
<5
-
<5
-
-
-
9
608
-
-
-
2,700
500
750
—
-
-
-
-
—
548
>147
-
<5
200
-
<7
-
-
88
672
1,080
-
-
<5
12
<5
-
<5
-
-
-
13
906
—
-
—
3,400
390
570
—
-
-
-
— •
—
549
>147
-
<5
170
-
<7
-
-
57
553
962
-
-
7
9
<5
-
<5
-
-
-
10
698
-
-
-
3,000
490
700
••
-
-
-
—
—
550
>147
-
<5
150
-
<7
-
-
37
283
386
-
-
9
<5
<5
-
<5
-
-
—
3
187
••
-
-
420
<100
110
•*
-
-
-
••
•
551
>147
—
<5
100
-
<7
-
-
44
316
481
-
-
8
<5
<5
-
<5
-
-
-
8
206
—
-
-
1,700
340
540
—
—
-
-
—
—
552
>i47
-
<5
140
-
<7
-
-
59
890
630
—
-
10
7
<5
-
<5
—
—
—
18
525
~
-
-
6,600
300
400
•
-
-
—
—
-
PNAs
Naphthalene
Penanthrene/ Anthracene
Pyrene
Benz o (a ) anthracene
Benzo(a)pyrene
Alkylbenzene (C.H.
Alkylnaphthaleni t
)
Chlorine, wt 2
Sulfur, ut 2
PCBs
0.47
0.48
12
0.46
0.47
10
0.40
0.42
11
0.39
0.37
6
0.46
0.46
10
0.14
0.22
<5
0.26
0.26
5
0.49
0.29
* Table A-2 identifies the source of analytical data for each used oil sample. Table A-3 provides codes
for each sample number which describes the specific generating source of used oil and the end-use.
A-64
-------
TABLE A-l (continued)
ANALYTICAL DATA FOR USED OIL SAMPLES
Flash Point (°F)
Metals
Aluminum
Arsenic
Barium
Beryllium
Cadmium
Chromium
Cobalt
Copper
Iron
Lead
Magnesium
Manganese
Molybdenum
Nickel
Selenium
Silicon
Silver
Sodium
Tin
Titanium
Vanadium
Zinc
Volatile Organics
Dichlo rod! fluorome thane
Irichlorof luoromethane
Tr ichlorotr if luoroe thane
1 ,1 ,1-Trichloroethane
Tr ichloroe thy lene
Tetrachloroethylene
Phenol
Benzene
Toluene
Ethyl Benzene
Xylenes
Methylene Chloride
553
>147
-
<5
150
-
<7
-
-
105
3.530
745
-
-
7
13
<5
-
<5
-
-
-
44
629
-
-
-
1,400
<100
370
-
-
-
-
-
-
554
>147
-
16
<50
-
<7
-
-
57
2.840
301
-
—
<5
8
<5
-
<5
-
-
-
<5
405
-
-
-
450
<100
120
-
-
-
-
-
-
555
>147
-
<5
160
-
<7
-
-
82
695
673
-
-
5
9
<5
-
<5
-
-
-
8
627
-
»
-
1,900
310
500
-
-
-
-
-
-
Sample
556
>147
-
<5
150
-
<7
-
.
103
3,270
834
-
-
11
30
<5
-
<5
-
-
-
11
762
-
-
-
1.700
120
270
-
-
-
-
-
-
Number*
557
>147
-
<5
180
-
<7
-
-
61
2.000
471
-
-
9
14
<5
-
<5
-
-
-
31
383
-
-
-
11.000
320
260
-.
-
-
-
-
-
558 559
>147
-
<5
210
-
<7
-
-
99
3.060
643
-
-
7
23
<5
- -
9
-
-
-
32
712
-
-
-
9,600
270
220 -
-
-
-
-
-
-
560
>147
'_
<5
140
.
<7
-
_
115
1,510
872
-
-
<5
14
<5
-
<5
-
-
-
13
981
-
-
-
1.400
110
170
-
-
-
-
-
-
PNAS
Naphthalene
Penan threne /Anthracene
Pyrene
Benzo (a) anthracene
Benzo(a)pyrene
Alkylbenzene
Alkylnaphthalene tc
Phosphorus
. ,
J"
HI,)
Chlorine, wt %
Sulfur, wt %
PCBs
0
0
.26
.29
<2
0
0
.09
.12
2
0.
0.
27
29
6
0.27
0.28
<5
0.43
0.22
<2
0.37
0.28
0.
0.
6
19
33
5
* Table A-2 identifies the source of analytical data for each used oil sample. Table A-3 provides codes
for each sample number which describes the specific generating source of used oil and the end-use.
A-65
026G
-------
TABLE A-l (continued)
ANALYTICAL DATA FOR USED OIL SAMPLES
Sample Number*
Flash Point (°F)
Metals
Aluminum
Arsenic
Barium
Beryllium
Cadmium
Chromium
Cobalt
Copper
Iron
Lead
Magnesium
Manganese
Molybdenum
Nickel
Selenium
Silicon
Silver
Sodium
Tin
Titanium
Vanadium
Zinc
561
142
-
<5
150
-
<7
-
-
49
596
512
-
-
13
6
<5
-
<5
-
-
-
9
388
562
>147
-
<5
200
-
<7
-
-
54
495
931
-
-
12
7
<5
-
<5
-
-
-
15
650
563 564
>147
- —
<5
210
-
<7
-
-
99
3.060
643
-
—
7
23
<5
- -
9
-
-
- -
32
712
565 566
>U7
- -
<5
140
-
<7
-
-
115
1.570
872
-
- -
<5
14
<5
- -
<5
-
-
- -
13
981
567
141
-
<5
150
-
<7
-
-
49
596
512
-
-
13
6
<5
-
<5
-
-
-
9
388
566
>141
.,
_
<5
200
-
<7
-
-
54
495
931
-
-
12
7
<5
-
<5
-
-
-
15
650
Volatile Organics
Dichlorodifluoromethane
Trichlorofluoromethane
Trichlorotrifluoroethane
1,1,1-Trichloroethane
Trichloroethylene
Tetrachloroethylene
Phenol
Benzene
Toluene
Ethyl Benzene
Xylenes
Methylene Chloride
1,600
<100
990
4,200
720
900
9,600
270
220
1.400
110
170
1.600 4.200
<100 720
990 900
PNAs
Naphthalene
Penanthrene/Anthracene
Pyrene
Benzo(a)anthracene
Benzo(a)pyrene
Alkylbenzene (C.H,,)
Alkylnaphthalene TC.-H)
Phosphorus
Chlorine, wt X
Sulfur, wt Z
PCBs
0.18
0.25
<2
0.42
0.37
12
0.38
0.28
0.19
0.33
6 <5 5
0.18
0.25
<2
0.42
0.37
12
* Table A-2 identifies the source of analytical data for each used oil sample. Table A-3 provides codes
for each sample number which describes the specific generating source of used oil and the end-use.
A-66
-------
Sample Somber*
569 570 571 572 573 574 575 576
Flash Point (*F)
Metals
Aluminum
Arsenic
Barium
Beryllium
Cadmium
Chromium
Cobalt
Copper
Iron
Lead
Magnesium
Manganese
Molybdenum
Nickel
Selenium
Silicon
Silver
Soaiua
Tin
Titanium
Vanadium
Zinc
Volatile Organics
Dichlorodifluoromethane
Trichlorofluoromethane
Trichlorotrifluoroethane
1,1,1-Trichloroethane
Trichloroe:h\ lene
Tetrachloroethylene
Phenol
Benzene
Toluene
Ethyl Benzene
Xylenes
Methylene Chloride
PNAs
Naphthalene
Penanthrene /Anthracene
Pyrene
Benzo(a)anthracene
Benzo(a)pyrene
Alkylbenzene (CgH..,)
Alkylnaphthalene
Phosqhorus
. Chlorine, wt 7.
Sulfur, vt '/.
PCBs
16 10 14 13 10 14 12 11
* Table A-2 identifies the source of analytical data for each used oil sample. Table A-3 provides codes
for each sample number which describes the specific generating source of used oil and the end-use.
A-67
0267
-------
ANALYTICAL DATA FOR USED OIL SAMPLES
Flash Point (°F)
Metals
Aluminum
Arsenic
Barium
Beryllium
Cadmium
Chromium
Cobalt
Copper
Iron
Lead
Magnesium
Manganese
Molybdenum
Nickel
Selenium
Silicor.
Silver
Sodium
Tin
Titanium
Vanadium
Zinc
Volatile Organics
Dichlorod if luorome thane
Trichlorof luoromethane
Trichlorotrifluoroethane
1,1 , i-Iricnioroethatifc
Trichloroethylene
Tetrachloroethylene
Phenol
Benzene
Toluene
Ethyl Benzene
Xylenes
Methylene Chloride
577 578 579
126
- 20
- _ _
- - 80
_
- - -
- - 10
-. _ -
- 30
170
950
180
10
- - 10
- - <10
_
120
- - <10
790
<10
_ - -
• <10
600
- - -
- - -
_ _ _
310
160
. -
- 16
-
_
_
_
- - -
Sample Number*
580 581
263
10 10
- -
290 40
-
- -
<10 10
— -
30 <10
150 470
1.370 100
350 10
10 <10
10 <10
<10 10
- -
40 10
<10 <10
110 30
<10 <10
- -
<10 <10
1.130 30
- -
_ _
— -
130 7.5
-
6.9
8.8
- —
-
-
-
- -
582
145
<10
<1
60
<1
-
<10
-
10
40
680
90
10
10
<10
5
10
<10
80
<10
-
20
580
—
—
-
2.260
150
194
16
—
-
-
-
—
583
92
20
-
40
-
-
10
-
60
60
650
230
10
^10
^10
-
40
<10
130
<10
-
<1Q
770
—
-
—
360
19
93
18
—
—
-
-
—
584
-
<10
-
50
-
»
<10
-
20
50
650
40
10
<10
<10
-
10
<10
30
<10
-
<10
470
-
—
-
380
<100
-
47
—
-
-
-
—
PNAs
Naphthalene
Penanthrene/Anthracene
Pyrene
Benzo(a)anthracene
Benzo(a)pyrene
Alkylbenzene (Co
Alkylnaphthalenl
Phosphorus
Chlorine, wt %
Sulfur, wt %
PCBs
12 8.8
0.42
15
0.27
1.6
1.55
<1
* Table A-2 identifies the source of analytical data for each used oil sample. Table A-3 provides codes
for each sample number which describes the specific generating source of used oil and the end-use.
A-68
-------
TABLE A-l (continued)
ANALYTICAL DATA FOR USED OIL SAMPLES
Sample Number* t
Flash Point (°F)
Metals
Aluminum
Arsenic
Barium
Beryllium
Cadmium
Chromium
Cobalt
Copper
Iron
Uad
Magnesium
Manganese
Molybdenum
Nickel
Selenium
Silicon
Silver
Sodium
Tin
Titanium
Vanadium
Zinc
585^
105
20
40
120
750
120
10
150
830
10
330
566
145
30
20
50
140
510
30
380
<10
<10
670
587
160
50
10
30
1.600
250
380
160
20
4
1,000
380
10
100
190
588
210
90
50
10
30
30
40
30
120
589
68
10
60
10
160
3.250
320
10
10
10
20
10
590
190 1,190
591
138
15
177
18
220
18,500
410
17
59
1.350
592 (110)
> 200
, 22
<5.0
110
<0.2
1.4
4.2
0.5
180
270
240
34
3.4
51
<0.2
240
Oichiorodifluoromethane
Trichlorofluorooethane
Trichlorotrifluoroethane
1,1,1-Trichloroethane
Trichloroethylene
Tetrachloroethylene
Phenol
Benzene
Toluene
Ethyl Benzene
Xylenes
Mechvlene Chloride
580 17,400
350 234
950
32 43
160
190
300
19
840
<100
<2
590
16
10,000
<3
- <3
<3
<3
51
24
400
PSAs
Naphthalene
Penanthrene/Anthracene
Pyrene
Benzo(a)anthracene
Benzo(a)pyrene
Alkylbenzene (Cn
Alkylnaphthalene
Phosphorus
Chlorine, wt %
Sulfur, wt %
PCBs
12
6.4
0.16
580
0.43 -
0.50
11
0.86 -
0.54
240
0.06
0.29
<5
* Table A-2 identifies the source of analytical data for each used oil sample. Table A-3 provides codes
for each sample number which describes the specific generating source of used oil and the end-use.
t Numbers in parentheses represent EPA sample numbers for used oil samples obtained as part of their
1983 sampling program.
A-69
0268
-------
TABLE A-l (continued)
ANALYTICAL DATA FOR USED OIL SAMPLES
Flash Point (°F)
Metals
Aluminum
Arsenic
Barium
Beryllium
Cadmium
Chromium
Cobalt
Copper
Iron
Lead
Magnesium
Manganese
Molybdenum
Nickel
Selenium
Silicon
Silver
Sodium
Tin
Titanium
Vanadium
Zinc
Volatile Organics
Dichlorodifluoromethane
Trichlorofluoromethane
Trichlorotrifluoroethane
1,1,1-Trichloroethane
Trichloroethylene
Tetrachloroethylene
Phenol
Benzene
Toluene
Ethyl Benzene
Xylenes
Methylene Chloride
Sample Number*!
593 (111)594 (112)595(118) 596(119) 597(120) 598(121) 599(122) 600(123)
>200 <70 182 >200 <75 184 166 166
11
<5.0
2.2
<0.2
0.88
<0.5
150
110
6.4
170
1.5
<1.0
11
<5.0
38
<0.2
4.1
<0.5
49
140
330
250
5.4
1.3
19
<5.0
77
<0.2
1.7
0.52
29
280
1.800
290
11
1.3
<1.0
<5.0
0.67
<0.2
<0.5
<0.5
5.2
1.6
<5.0
0.79
<0.2
<1.0
13
<5.0
100
<0.2
1.1
<0.5
39
150
920
380
6.6
1.8
11
<5.0
93
<0.2
1.9
40
• L
<0.5
51
160
1,200
500
5.5
1.2
10
<5.6
38
<0.2
1.1
6 ft
• U
<0.5
32
150
3,000
450
9.1
1.2
" 12
<5.0
81
<0.2
1.1
3*
.j
<0.5
32
130
1,100
Z80
5-1
2.9
66
110
180
7.1 240
120
290
0.73 0.23 <0.2 <0.2 <0.2 <0.2 <0.2 4.3
280 1,100 1,100 68 1,100 1,100 1,000 780
<5
<5
<5
59
2.90
<5
190
<5
<4
<4
<4
3,600
6,500
510
14,000
<4
<16
<16
<16
73
290
440
1,100
<16
<4
<4
<4
<4
<4
<4
17
<4
<5
<5
8.6
<5
97
69
600
<5
<8
<8
<8
<8
150
<8
280
<8
<3
<3
<3
<3
60
110
220
<3
82
<5
<5
<5
72
86
500
<5
PNAS
Naphthalene
Penanthrene/Anthracene
Pyrene
Benzo(a)anthracene
Benzo(a)pyrene
Alkylbenzene (C.H.,)
Altcylnaphthalene tt.-H.,)
Phosphorus
Chlorine, wt Z
Sulfur, wt %
PCBs
0.
0.
<5
01
37
0.
0.
<5
04
39
0.
0.
<5
08
40
0.01
0.30
<5
0.10
0.41
<5
0.07
0.37
<5
0.15
0.68
<5
0.13
0.48
<5
* Table A-2 identifies the source of analytical data for each used oil sample. Table A-3 provides code;
for each sample number which describes the specific generating source of used oil and the end-use.
t Numbers in parentheses represent EPA sample numbers for used oil samples obtained as part of their
1983 sampling program.
A-70
-------
TABLE A-l (continued)
ANALYTICAL DATA FOR USED OIL SAMPLES
Flash Point (°F)
Mecals
Aluminum
Arsenic
Barium
Beryllium
Cadmium
Chromium
Cobalt
Copper
Iron
Lead
Magnesium
Manganese
Molybdenum
Nickel
Selenium
Silicon
Silver
Sodium
Tin
Titaniun
Vanadium
Zinc
Volatile Organics
Diehlorodifluoromethane
Trichlorofluoromethane
Trichlorotrifluoroethane
1,1,1-Trichloroethane
Trichloroeth>lene
Tetrachloroethylene
Phenol
Ber.zer.e
Toluene
Ethyl Benzene
Xylenes
Methylene Chloride
Sample Number*!
601(125) 6(12(126) 603(127) 604(128) 605(129) 606(130) 607(131) 608(132)
>200
94
188
>200
186
84
186
>200
4.9
<5.0
8.1
<0.2
1.0
1C
.3
<0.5
48
100
78
330
3.0
12
5.9
19
<0.2
1.4
20
.0
<0.5
100
360
20
84
3.1
8.6
<5.0
48
<0.2
0.52
90
• J
0.98
35
100
83
170
2.0
33
<5.0
95
<0.2
0.63
<0.5
200
200
140 1.
51
3.0
<5.0
640
<0.2
1.4
0.58
37
170
900 2
450
9.9
13
<5.0
160
<0.2
0.54
<0.5
30
84
.300 2
230
8.3
17
<5.0
99
<0.2
1.6
<0.5
42
200
,000
420
9.9
" 5.6
<5.0
27
<0.2
<0.5
<0.5
20
37
200
250
1.8
1.8
200 160
1.2
1.1
1.3
56 170 160 160
1.9
89
<0.2 0.22 <0.2 <0.2 <0.2 <0.2 <0.2 <0.2
820 550 1,000 230 1.200 1.100 1.100 1.000
<3
<3
55
<3
39
16"
110
<3
<1
<1
12
<1
<1
12
120
4
<6
<6
420
<6
190
200
660
<6
<1
2
2
<1
14
19
43
<1
<6
<6
<6
15
1.500
590
1.900
190
520
<5
280
1.600
3,500
1.000
3,700
<5
<10
<10
<10
<10
1,300
2.200
11.000
<10
<8
<8
<8
110
410
150
490
<8
PNAS
Naphthalene
Penanthrene/Anthracene
Pyrene
Benzo(a)anthracene
Benzo(a)pyrene
Alkylbenzene (C-H.,)
Alkylnaphthalene TC...H..-)
Phosphorus
Chlorine, wt 2
Sulfur, wt %
PCBs
0.
0
<5
04
.86
.0
0.04
0.52
<5.0
0.10
0.54
<5.0
0.02
0.32
<5.0
0
0
<5
.08
.53
.0
0.11
0.51
<5.0
0.08
0.47
<5.0
0
0
<5
.02
.56
.0
* Table A-2 identifies the source of analytical data for each used oil sample. Table A-3 provides codes
for each sample number which describes the specific generating source of used oil and the end-use.
* Numbers in parentheses represent EPA sample numbers for used oil samples obtained as part of their
1983 sampling program.
A-71
02G(J
-------
TABLE A-l (continued)
ANALYTICAL DATA FOR USED OIL SAMPLES
Sample Number *t
Flash Point (°T)
Metals
Aluminum
Arsenic
Barium
Beryllium
Cadmium
Chromium
Cobalt
Copper
Iron
Lead
Magnesium
Manganese
Molybdenum
Nickel
Selenium
Silicon
Silver
Sodium
Tin
Titanium
Vanadium
Zinc
609 (133)610(135) 611(137) 612(138) 613(140) 614(142) 615(146) 616(147)
138 >200 85 >200 <80 124 >200 >200
16
<5
71
<0
1
6
<0
56
170
1,600
550
8
-
1
-
-
-
130
-
-
<0
850
.0
.2
.3
.6
.5
.0
.2
.2
*1.0
<5.0
0.61
<0.2
<0.5
<0.5
<0.5
0.64
<1.0
<5.0
<0.5
<0.2 •
-
<1.0
-
-
-
<1.0
-
-
<0.2
8.7
6
<5
37
<0
<0
0
<0
9
32
280
13
1
-
<1
-
-
-
1
-
-
0
380
.7
.0
.2
.5
.52
.5
.8
.3
.0
.9
.27
1.6
<5.0
20
<0.2
<0.5
<0.5
Chlorine, wt %
Sulfur, wt %
PCBs
0
0
<5
.14
.44
.0
0.22
0.25
13
0.10
0.47
<5
0.10
0.56
<5
0.29
0.44
<5
0.15
0.42
<5
0.02
0.68
<5
0.
0,
<5
.05
.54
* Table A-2 identifies the source of analytical data for each used oil sample. Table A-3 provides codes
for each sample number which describes the specific generating source of used oil and the end-use.
+ Numbers in parentheses represent EPA sample numbers for used oil samples obtained as part of their
1983 sampling program.
A-72
-------
TABLE A-l (continued)
ANALYTICAL DATA FOR USED OIL SAMPLES
Flash Point (°F)
Metals
Aluminum
Arsenic
Barium
Beryllium
Cadmium
Chromium
Cobalt
Copper
Iron
Lead
Magnesium
Manganese
Molybdenum
Nickel
Selenium
Silicon
Silver
Sodium
Tin
Titanium
Vanadium
Zinc
Volatile Organics
Dichlorodifluoromethane
Trichlorofluoromethane
Trichlorotrifluoroethane
1,1.1-Trichloroethane
Trichloroethylene
Tetrachloroethylene
Phenol
Benzene
Toluer.e
Ethyl Benzene
Xylenes
Methvlene Chloride
Sample Number*t
617 (US) 618(151) 619(152) 620(161) 621(164) 6_2j(165) 623(165) 624(166)
<70
90
106
>200
96
196
124 >200
7.7
<5.0
5.3
<0.2
0.78
1.0
<0.5
43
80
130
7.6
2.3
<1.0
11
*5.0
16
<0.2
0.9
3.2
<0.5
39
71
390
370
3.8
" <1.0
9.8
<5.0
18
<0.2
0.84
3.7
<0.5
44
68
340
60
7.8
1.5
19
<5.0
0.9
<0.2
<0.5
<0.5
<0.5
<0.5
26
<5.0
17
0.23
19
3.9
<5.0
66
<0.2
<0.5
7.4
0.94
9.8
130
130
4.7
1.1
1.6
160
<5.0
21
<0.2
<0.5
5.1
1.8
16
640
17
76
4.3
26
3.3
<5.0
4.3'
<0.2
0.59
1.1
<0.5
15
88
200
10
1.3
" <1.0
410
" <5.0
14
<0.2
<0.5
10
6.2
16
630
59
6.3
5.6
17
5.6
69
12
110
45
68
14
10
<0.2
380
29
<20
<20
260
580
1,600
1,700"
<20
<0.2
790
1,300
<12
260
210
770
1.200
3.500
<12
<0.2
670
16
<10
<10
950
1,000
710
1.300
810
80
8.8
<12
<12
<12
890
500
320
620
<12
3.2
170
210
<9
35
300
15,000
300
3.000
140
92
190
<12
<12
<12
220
780
140
580
<12
0.
260
<9
<9
<9
650
1,100
680
1.100
<9
28 0.32
63
1.900
1.400
1.100
210
850
210
1.400
27
PSAs
Naphthalene
Penanthrene/Anthracene
Pyrene
Benzo(a)anthracene
Benzo(a)pyrene
Alkylbenzene (Cgll.,)
Alkylnaphthalene tc H )
Phosphorus
Chlorine, vt %
Sulfur, wt %
PCBs
-
0.09
°<538
-
0.12
<°5'46
-
0.06
0.18
<5
— -
0.04
1.33
<5
0.25
0.86
-
0.06
1.55
<5
—
0.05
0.41
<5
—
0.61
0.45
30
* Table A-2 identifies the source of analytical daca for each u«ed oil sample. Table A-3 provides codes
for each sample number which describes the specific generating source of used oil and the end-use.
t Numbers in parentheses represent EPA sample numbers for used oil samples obtained as part of their
1983 sampling program.
A-73
0270
-------
TABLE A-l (continued)
ANALYTICAL DATA FOR USED OIL SAMPLES
Flash Point (°F)
Metals
Aluminum
Arsenic
Barium
Beryllium
Cadmium
Chromium
Cobalt
Copper
Iron
Lead
Magnesium
Manganese
Molybdenum
Nickel
Selenium
Silicon
Silver
Sodium
Tin
Titaniun
Vanadium
Zinc
Volatile Organics
Dichlorodifluoromethane
Trichlorofluoromethane
Trichlorotrifluoroethane
1,1,1-Trichloroethane
Trichloroethylene
Tetrachloroethylene
Phenol
Benzene
Toluene
Ethyl Benzene
Xylenes
Methvlene Chloride
Sample Humbert
625(167)626(168)627(169)628(170)629(174) 630(177)631(181)632(182)
>200
• 200
>200
>200
>200
140
>200 - -
180
<5.0
2.6
<0.2
<0.5
5.2
1.4
1.9
240
6.9
2.5
2.3
12
440
<5.0
38
0.2
<0.5
1.2
0.56
12
210
48
26
3.5
1.2
76
<5.0
19
<0.2
<0.2
7.4
3.3
1.6
190
31
3.1
4.6
24
65
<5.0
17
<0.2
<0.5
5.9
3.4
0.7
140
22
2.1
3.8
24
43
<5.0
2.5
<0.2
<0.5
4.9
<0.69
7.4
180
6.9
<0.5
0.73
8.3
1.2
<5.0
50
<0.2
<0.5
<0.5
<0.5
4.9
52
57
11
0.88
<1.0
120
<5.0
16
<0.2
<0.5
2.6
0.8
8.3
380
11
41
3.2
18
86
<5.0
12
<0.2
<0.5
2.2
0.59
6.2
330
10
29
2.6
18
5.0 340
6.1
1.1 <1.0 <1.0 46
38
<8
49
17
190
85
76
<8
580
160
44
32
83
21
260
240
140
98
160
15
17
75
48
400
290
280
930
320
1,200
35
0.21 0.28 0.46 0.49 <0.2 0.95 110 110
40 170 88 78 20 210 78 66
<8
<8
<8
12
47
<8
74
<8
PNAs
Naphthalene
Penanthrene/Anthracene
Pyrene
Benzo(a)anthracene
Benzo(a)pyrene
Alkylbenzene (C.H-,)
Alkylnaphthalenfe tcH)
Chlorine, wt Z
Sulfur, wt Z
PCBs
0.37
0.26
<5
0.47
0.09
<5
0.15 -
0.20 -
<5 23
0.61
0.86
12
0.03
0.43
<5
0.15
0.94 -
<5
0.09
<5
* Table A-2 identifies the source of analytical data for each used oil sample. Table A-3 provides codes
for each sample number which describes the specific generating source of used oil and the end-use.
+ Numbers in parentheses represent EPA sample numbers for used oil samples obtained as part of their
1983 sar.pling program.
A-74
-------
TABLE A-l (continued)
ANALYTICAL DATA FOR USED OIL SAMPLES
Flash Point (°F)
Metals
Aluminum
Arsenic
Barium
Beryllium
Cadmium
Chromium
Cobalt
Copper
Iron
Lead
Magnesium
Manganese
Molybdenum
Nickel
Selenium
Silicon
Silver
Sodium
Tin
Titanium
Vanadium
Zinc
Volatile Organics
Dichlorodifluoromethane
Trichlorofluoromethane
Trichlorotrifluoroethane
1,1,1-Trichloroethane
Trichloroethylene
Tetrachloroethylene
Phenol
Benzene
Toluene
Ethyl Benzene
Xylenes
Methvlene Chloride
Sample Number*t
633(187)634(188) 635(190)636(191)637(193)638(202)639(204)640(205)
>200 116 138 184 178 >200 >200 >200
100
<5.0
33
<0.2
1.8
64
1.5
120
500
76
230
23
16
<5.0
38
<0.2
<0.5
13
1.4
1.1
300
37
84
25
31
<5.0
32
<0.2
<0.5
16
1.6
6.1
620
55
36
16
3.1
<5.0
120
<0.2
<0.5
<0.5
<0.5
21
15
5.1
1.5
0.34
23
<5.0
46
<0.2
<0.5
4.3
<0.5
70
410
190
<0.5
0.34
13
<5.0
33
<0.2
<0.5
1.0
<0.5
0.52
110
<5.0
1.6
0.32
1.3
<5.0
<0.5
<0.2
<0.5
<0.5
<0.5
110
18
6.8
0.82
0.30
,4.9
-------
TABLE A-l (conttnu+d)
ANALYTICAL DATA FOR USED OIL SAMPLES
Flash Point (°F)
Metals
Aluminum
Arsenic
Barium
Beryllium
Cadmium
Chromium
Cobalt
Copper
Iron
Lead
Magnesium
Manganese
Molybdenum
Nickel
Selenium
Silicon
Silver
Sodium
Tin
Titanium
Vanadium
Zinc
Volatile Organics
Dichlorodifluoromethane
Trichlorofluoromethane
Trichlorotrifluoroethane
1,1.1-Trichloroethane
Trichloroethylene
Tetrachlorfiethylene
Phenol
Benzene
Toluene
Ethyl Benzene
Xylenes
Methylene Chloride
Sample Number*!'
6^1(207) 642(208) 643(209) 644(233) 645(242) 646(243) 647(245) 6_4_8(2SO)
>200 136 164 138 >200 >200 112 >200
72
<5.0
21
<0.2
<0.5
1.8
<0.5
42
76
X80
68
3.4
2.9
<5.0
4.3
<0.2
<0.5
3.8
<0.5
4.3
120
80
8.2
1.9
4.1
<5.0
1.9
<0.2
<0.5
1.6
<0.5
1.7
62
48
16
1.1
57
<5.0
130
<0.2
<0.5
1.2
<0.5
1.1
200
10
5.8
1.6
<1.0
<5.0
3.1
<0.2
0.5
<0.5
<0.5
5.2
1.5
<5.0
<0.5
<0.2
20
<5.0
3.1
<0.2
1.2
5.1
0.72
47
280
2.000 2
460
19
14 .,
<5.0
8.7
<0.2
3.5
4.2
<0.5
9.1
170
.700
410
27
1.7
<5.0
17
<0.2
1.1
0.57
<0.5
24
82
ISO
16
4.7
11
100
12
25
53
4.2 <1.0
1.8
1.2 <1.0
68
<1.0 200
120
9.9
38 0.44 68
180 80 58
2.1 <0.2 <0.2 <0.2 <0.2
8.3 210 1-.200 1.100 390
180
140
120
110
420
660
1,200
45
<13
38
27
30
600
180
810
<13
<7
<7
<7
<7
150
89
410
<7
<6
<6
<6
<6
60
<6
300
<6
<4
<4
<4
<4
6,300
<4
-------
TABLE A-l (continued)
ANALYTICAL DATA FOR USED OIL SAMPLES
Flash Point (°F)
Metals
Aluminum
Arsenic
Barium
Berylliua
Cadmium
Chromium
Cobalt
Copper
Iron
Lead
Magnesium
Manganese
Molyoaenun
Nickel
Selenium
Silicon
Silver
Sodium
Tin
Vanadium
Zinc
Volatile Organics
Dichlorodifluoromethane
Trichlorofluoromethane
Trichlorotrifluoroethane
1,1,1-Trichloroethane
Trichloroechylene
Tetrachloroethylene
Phenol
Benzene
Toluene
Ethyl Benzene
Xylenes
Methvlene Chloride
Sample Number*f
649(255)650(256) 651(257)652(258)653(259)654(261)655(265)656(267)
172 >200 >200 >200 >200 >200 >200 ">200
19
<5.0
14
<0.2
<0.5
2.1
1.2
4.0
68
140
14
2.5
50
<5.0
16
<0.2
0.58
2.9
0.55
2.1
270
370 1
30
6.5
13
<5.0
110
<0.2
1.3
5.9
<0.5
29
170
,500
360
12
20
<5.0
4.2
<0.2
1.6
8.2
<0.5
17
310
1,200
550
9.9
19
<5.0
4.3
<0.2
1.8
8.1
<0.5
17
320
1,200
560
9.8
23
<5.0
2.8
<0.2
2.1
8.4
<0.5
17
320
1,400
470
12
220
<5.0
4.1
<0.2
<0.5
3.0
<0.5
3.3
99
24
3.8
3.2
<1.0
<5.0
<0.5
<0.2
<0.5
<0.5
<0.5
21
3.1
<5.0
<0.5
<0.2
16
19
19
80
2.0
27
1.7
73
1.9
2.1
320
270
2.1
84
0.35 <0.2 <0.2 <0.2 <0.2
300 1,200 1,100 1,100 1,200
170
440
37
40
11
230
190
970
<4
<4
<4
<4
57
130
550
<4
<16
<16
46
460
230
990
<16
<16
<16
60
710
180
1,200
<16
<15
<15
130
670
460
1,500
<15
5.2
<0.2
26
470
<0.2
400
<8
<8
<8
<8
<8
<8
<8
<8
PNAs
Naphthalene
Penanthrene/Anthracene
Pyrene
Benzo(a)anthracene
Benzo(a)pyrene
Alkylbenzene (C
Alkylnaphthalene
Phosphorus
Chlorine, vt Z
Sulfur, wt '/,
PCBs
0.09
0.80
<5
0.91
0.43
<5
1.200
0.06
0.56
<6
1,000
0.02
0.53
<5
1,000
0.03
0.53
<5
0.05
0.60
<5
0.
0.
<5
20
35
<0.
0.
<5
01
30
* Table A-2 identifies the source of analytical data for each used oil sample. Table A-3 provides codes
for each sample number which describes the specific generating source of used oil and the end-use.
t Numbers in parentheses represent EPA sample numbers for used oil samples obtained as part of their
1983 sampling program.
A-77
0272
-------
TABLE A-l (continued)
ANALYTICAL DATA FOR USED OIL SAMPLES
Sample Number *t
657(268) 658(271) 659(272) 660
Flash Point CF)
Metals
Aluminum
Arsenic
Barium
Beryllium
Cadmium
Chromium
Cobalt
Copper
Iron
Lead
Magnesium
Manganese
Molybdenum
Nickel
Selenium
Silicon
Silver
Sodium
Tin
Titanium
Vanadium
Zinc
Volatile Organics
Dichlorod if luorome thane
Trichlorof luoromethane
Trichlorotrif luoroethane
1 ,1 ,1-Trichloroethane
Trichloroethylene
Tetrachloroethylene
Phenol
Bcr.zcric
Toluene
Ethyl Benzene
Xylenes
Methylene Chloride
PSAs
Naphthalene
Penanthrene /Anthracene
Pyrene
Benzo (a ) anthracene
Benzo(a)pyrene
>200
<1.0
<5.0
18
<0.2
<0.5
<0.5
<0.5
<0.5
120
<5.0
2.5
10
-
1.0
-
-
-
4.3
-
-
<0.2
19
-
-
-
<15
<15
<15
-
<15
200
4
<5
13
<0
0
3
<0
20
85
500
700
4
-
<1
-
-
-
59
-
-
<0
1,100
-
-
-
110
<4
180
-
<4
53
43
170
<4
-
-
-
-
-
128
.8 52
.0 <1.0
51
.2 0.2
.73 0.8
.5 17
.5 1.0
19
490
1,070
43
.9 10
2.5
.0 12
<0.4
26
<0.3
24
2.6
1.3
.2 11
170
<20
<100
230
14,000
1.600
13.000
70
<100
9,700
330
1,300
<20
990
260
30
35
<5
6_61
104
15
10
70
0.1
1.6
3.8
1.0
34
150
1,170
190
6.4
3.6
2.3
<0.4
20
<0.1
130
7.9
0.8
0.6
690
<30
<30
<30
2,000
- 370
640
40
<100
3,100
3.700
2,600
<30
430
100
30
12
<5
662
116
1.5
0.9
84
<0.1
0.2
1.2
0.3
12
84
170
4.6
1.2
0.4
0.6
<0.4
<0.1
<0.1
14
<0.7
<0.1
0.9
91
<30
<30
860
500
730
<90
<5
<30
380
560
3,300
<30
1,400
330
20
10
<5
663
-
17
6.2
32
«0.1
1.5
4.8
0.2
36
170
810
300
11
7.6
15
<0.4
41
<0.1
160
11
7.0
0.3
890
<20
<20
1,900
880
3,700
620
35
100
4,400
570
1,800
<20
230
80
15
30
<5
664
-
47
6.2
54
0.9
0.8
5.4
0.4
40
200
810
210
7.6
3.4
7.6
<0.4
35
<0.1
510
3.8
4.2
13
620
<20
<20
1,300
670
170
200
25
90
1,000
390
1,100
<20
750
390
70
60
<5
AlVcylbenzene (CgH
Alkylnaphthalene
42,000
<30
4,100
Chlorine, wt %
Sulfur, wt %
PCBs
• 0.
0.
<5
12
45
0.07
0.33
<5
0.06
0.63
<5
2.
0.
7
59
0.
0.
36
61
0.17
0.27
0.51
0.69
0.23
0.75
* Table A-2 identifies the source of analytical data for each used oil sample. Table A-3 provides codes
for each sample number which describes the specific generating source of used oil and the end-use.
t Numbers in parentheses represent EPA sample numbers for used oil samples obtained as part of their
1983 sampling program.
A-78
-------
TABLE A-l (continued)
ANALYTICAL DATA FOR USED OIL SAMPLES
Sample Number*t
Flash Point (°F)
Metals
Aluminum
Arsenic
Barium
Beryllium
Cadmium
Chromium
Cobalt
Copper
Iron
Lead
Magnesium
Manganese
Molybdenum
Nickel
Selenium
Silicon
Silver
Sodium
Tin
Titar.iur
Vanadium
Zinc
Volatile Orgar.ics
Dichlorodifluorome thane
Trichlorofluoromethane
Trichlorotrifluoroethane
1,1 ,1-Trichloroethane
Trichloroethylene
- Tetrachloroethylene
Phenol
Benzene
Toluer.e
Ethyl Benzene
Xylenes
Methylene Chloride
PNAs
Naphthalene
Penanthrene /Anthracene
Pyrene
Benzo (a) anthracene
Benzo(a)pyrene
665
104
11
7
30
<0
1
3
0
19
100
950
78
5
2
3
<0
19
<0
250
4
1
3
430
<30
<30
940
840
<100
190
<5
190
12,000
1,500
6,400
<30
990
380
40
<5
<5
.1
.1
.0
.3
.2
.6
.3
.0
.4
.1
.3
.5
.1
^
666
200
13
5.0
71
<0.1
1.3
4.0
<0.1
45
120
660
430
7.3
2.9
1.8
<0.4
20
<0.1
85
3.9
1.1
<0.1
850
<20
<20
<20
110
<20
210
<5
<90
510
180
650
<20
210
80
<5
<5
<5
667
108
15
8.
64
<0.
1.
4.
<0.
37
150
1,800
280
8.
3.
1.
<0.
12
<0.
100
8.
1.
0.
1.050
<20
<20
620
390
<90
610
18
190
3,500
840
3,400
<20
420
100
42
25
7
8
1
4
9
1
4
9
7
4
1
5
0
1
668
172
20
7.4
100
<0.1
1.2
4.4
0.1
32
160
1.500
280
7.5
3.7
1.5
<0.4
20
<0.1
170
7.8
1.3
0.1
900
<30
<20
380
310
<90
490
14
170
2,500
670
2,500
<20
340
100
35
8
<5
669
-
640
4.5
84
0.4
1.0
18
0.2
130
1,300
350
240
28
13
86
<0.4
200
<0.1
450
17
21
7.5
340
<30
<30
1,400
1,700
790
690
45
<100
1,400
440
1,400
<30
270
150
20
20
<5
670 (13)671_ (14) 672
94
9
<5
4
<0
«0
2
5
0
46
13
13
1
-
3
-
-
-
<1
-
-
12
6
-
-
-
<11
<11
230
-
6,900
4,800
2.000
4,000
<11
-
-
-
—
<75
.4 13
<5
.4 3
.2 <0.2
.5 <0.5
.4 2.0
<0.5
.52 1.9
180
<5
6.3
.0 1.3
-
.9 6.4
-
-
-
6.2
-
-
24
.6 5.8
-
-
-
<70
<70
<70
-
2,700
1,800
1,100
3,100
<70
:
-
—
~
92
•' 9
<5
4
<0
<0
2
5
0
49
13
13
1
-
3
-
-
-
<1
-
-
12
6
-
-
-
<33
<33
<33
-
8,200
6,000
1,000
5,100
<33
:
—
—
*
(15)
.9
.8
.2
.5
.5
.54
.1
.7
.9
Alkylbenzene (CQIL )
.11 i __ i i i •* -vrf
<30 36,000
<20
<30
Phosphorus
Chlorine, wt %
Sulfur, wt %
PCBs
----- 52
0.18 0.25 0.12 0.11 0.34 0.03
0.36 0.66 0.62 0.65 0.67 1.00
- <5
12
0.06
0.55
<5
48
0.03
1.24
<5
* Table A-2 identifies the source of analytical data for each used oil sample. Table A-3 provides codes
for each sample number which describes the specific generating source of used oil and the end-use.
+ Numbers in parentheses represent EPA sample numbers for used oil samples obtained as part of their
1983 sampling program.
A-79
0273
-------
TABLE A-l (continued)
ANALYTICAL DATA FOR USED OIL SAMPLES
Flash Point (°F)
Mecals
Al uminum
Arsenic
Barium
Beryllium
Cadmium
Chromium
Cobalt
Copper
Iron
Lead
Magnesium
Manganese
Molybdenum
Nickel
Selenium
Silicon
Silver
Sodium
Tin
Titanium
Vanadium
Zinc
Volatile Organics
Dichlorodifluoromethane
Trichlorofluoroaethane
Trichlorotrifluoroethane
1,1,1-Trichloroethane
Trichloroethylene
Tetrachloroethylene
Phenol
Benzene
Toluene
Ethyl Benzene
Xylenes
Mechylene Chloride
Sample Number*t
673 ^16)674 (60)675U04.) 676(105) 677(106) 678(107) 679(108) 680(109)
-.75 >200 188 >200 >200 >200 >200 188
2.0
<5
2.5
<0.2
<0.5
<0.5
<0.5
<0.5
35
<5
2
0.51
5.5
20
<5
38
<0.2
1.6
6.1
<0.5
55
220
2.300
370
17
19
<5
50
<0.2
1.5
7.0
<0.5
22
260
1,400
68
14
14
<5
49
<0.2
1.4
4.7
<0.5
44
160
1,000
230
13
12
<5
11
<0.2
1.2
4.4
1.1
32
180
1,300
280
16
11
<5
34
<0.2
1.3
4.1
0.87
25
140
1,000
130
14
13
<5
23
<0.2
1.3
4.4
<0.5
29
170
1,000
410
12
9.5
<5
15
" <0.2
1.1
3.1
<0.5
37
120
720
97
6.2
1.2
63
26
100
180
70
91
36
17 <0.2 <0.2 <0.2 <0.2 <0.2 <0.2 <0.2
8.2 1.100 880 910 960 710 1,000 830
<60
<60
<60
<60
18,000
<60
1,300
<60
<9
<9
<9
<9
460
170
"490
<9
2.100
240
73
340
400
900
37
23
96
260
36
790
16
170
530
440
640
150
250
330
650
<21
<21
79
160
800
2.000
320
120
480
280
2,300
23
PNAs
Naphthalene
Penanthrene/Anthracene
Pyrene
Benzo(a)anthracene
Benzo(a)pyrene
Alkylbenzene (CnH,-)
Phosphorus
Chlorine, wt Z
Sulfur, wt '/.
PCBs
11
0.
0.
<5
1,100
02 0.08
50 0.44
<5
870
0.19
0.46
<5
870
0.
0.
<5
05
46
950
0.
0.
<5
02
63
670
0.04
0.41
<5
900 2
0.06
0.74
<5
.400
0.
0.
<5
10
45
* Table A-2 identifies the source of analytical data for each used oil sample. Table A-3 provides codes
for each sample number which describes the specific generating source of used oil and the end-use.
t Numbers In parentheses represent EPA sample numbers for used oil samples obtained as part of their
1983 sampling program.
A-80
-------
ANALYTICAL DATA FOR USED OIL SAMPLES
.•lash Point (°F)
Metals
Aluminum
Arsenic
Barium
Beryllium
Cadmium
Chromium
Cobalt
Copper
Iron
Lead
Magnesium
Manganese
Molybdenum
Nickel
Selenium
Silicon
Silver
Sodium
Tin
Iitar.iu=
Vanadium
Zinc
Volatile Organics
Dichlorodifluoromethane
Tr ichlorofluoromethane
Tr ic hlorocnf luoroe thane
1,1,1-Trichloroethane
Trichloroethyiene
letrachloroethylene
Phenol
Benzene
Toluene
Ethyl Ber.zene
Xvle-e-
Methylene Chloride
Sample Number*t
681(211) 682(212) 683(213) 684(218) 685UZO) 686(227) 687(228) 688(230)
146 92 >200 132 102 >200 168 144
3.8
<5.0
0.5
<0.2
<0.5
0.54
<0.5
1.9
80.0
<5.0
2.5
0.53
1.8
<5.0
1.2
<0.2
<0.5
0.97
<0.5
6.3
46.0
11.0
0.68
0.72
3.3
5.1
9.2
<0.2
<0.5
1.8
0.62
320.0
110.0
<5.0
13.0
5.0
<1.0
<5.0
<0.5
<0.2
<0.5
<0.5
<0.5
<0.5
<1.0
<5.0
<0.5
<0.2
<1.0
*^.o
4.0
<0.2
1.3
0.59
<0.5
19.0
1.3
<5.0
1.4
<0.2
*1.0
<5.0
2.6
<0.2
<0.5
<0.5
<0.5
0.55
150.0
<5.0
<0.5
4.6
<1.0
<5.0
<0.5
<0.2
<0.5
<0.5
<0.5
<0.5
4.6
<5.0
<0.5
<0.2
25.0
<5.0
32.0
<0.2
r.i
4.9
<0.5
52.0
210.0
910.0
95.0
10.0
11.0
7.5
<1.0 <1.0 2.5 <1.0 3.3 5.0
1.6
2.0 80.0
0.2 18.0 1.1 <0.2 <0.2 <0.2 <0.2 <0.2
1.8 36.0 460.0 <0.5 17.0 2.5 0.53 700.0
<7
<7
<7
<7
200
350
830
<7
<13
93
<13
540
12,000
8,400
20,000
570
<22
<22
<22
<22
120
32
350
<22
<7
<7
<7
<7
<7
<7
<7
<7
62,000
<11
<11
"<11
170
<11
26
5,100
230
3,400
860
81
340
2,000
1,200
1,700
PNAs
Naphthalene
Penanthrene/Anthracene
Pyrene
Benzo(a)anthracene
Ber.zo(a)pyrene
Alkylbenzene (CgH,,)
Phosptiorus
Chlorine, wt 7.
Sulfur, wt X
PCBs
<5.0
0.
0.
<5
15.0 180.
02 0.06
41 0.35
<5 <5
0 <5.0 130.
0.27 0.02
0.19 0.15
<5 <5
0
2.46
0.02
8.3
0.96
0.06
6.0 720.0
5.45 0.21
5.62 0.51
<5 <5
* Table A-2 identifies the source of analytical data for each used oil sample. Table A-3 provides codes
for each sample number which describes the specific generating source of used oil and the end-use.
t Numbers in parentheses represent EPA sample numbers for used oil samples obtained as part of their
1983 sampling program.
A-81
0274
-------
TABLE A-l (continued)
ANALYTICAL DATA FOR USED OIL SAMPLES
Flash Point (°F)
Metals
Aluminum
Arsenic
Barium
Beryllium
Cadmium
Chromium
Cobalt
Copper
Iron
Lead
Magnesium
Manganese
Molybdenum
Nickel
Selenium
Silicon
Silver
Sodium
Tin
Titanium
Vanadium
Zinc
Volatile Organics
Dichlorodifluoromethane
Trichlorofluoromethane
Trichlorotrifluoroethane
1,1,1-Trichloroethane
Trichloroethylene
Te trachloroe thylene
Phenol
Benzene
Toluene
Ethyl Benzene
Xylenes
Methylene Chloride
Sample Number*t
689(280) £90(281) 691(282) 692(284) 693(285) 694(288) 695(292) 696(294)
170 154 178 196 >200 98 >200 >200
16
<5
64
<0.2
1.5
3.6
0.82
51
160
960
300
7.3
15
<5
38
<0.2
1.6
3.2
<0.5
60
130
730
220
5.6
12
<5
1.9
<0.2
<0.5
0.97
<0.5
33
7.8
34
9.3
0.24
3.3
<5
9.9
<0.2
<0.5
0.86
<0.5
49
140
96
4.4
2.1
2.1
<5
3.8
<0.2
0.63
1.1
<0.5
8.5
58
110
36
0.97
14
<5
52
<0.2
1.1
2.9
<0.5
44
130
830
150
5.5
88
<5
260
<0.2
2.8
50
1.7
110
980
2,000
370
29
74
<5
170
<0.2
0.57
5.6
<0.5
110
510
740
300
20
1.2
1.2
120 110
<1
2.7
6.5
5.1
1.3
15
2.6
4.1 37 120 380 640
<0.3 1.8 <0.2 <0.2 16 2.1 5.3 4.3
820 600 26 380 180 610 1,600 630
8
<17
37
170
2,900
380
1,400
<17
160
<17
28
110
1,400
260
1,100
<17
<7
<7
53
<7
76
110
630
<7
<8
1,400
190
<8
84
<8
420
<8
310
. 3 <18
..3 150
1.3 2,300
1.3 690
,.3 3,300
1.3 1,200
I 3,600
1.3 <18
66
<25
<25
<25
300
92
530
<25
6.8
71
62
12
ISO
120
470
<4.1
PNAs
Naphthalene
Penanthrene/Anthracene
Pyrene
Benzo(a)anthracene
Benzo(a)pyrene
Alkylbenzene (C^IL.)
Phosphorus 2 TZ
Chlorine, wt %
Sulfur, wt %
PCBs
740
0.08
0.50
<5
730
0.06
0.36
<5
30
0.02
0.20
<5
440
0.48
0.59
<5
220
0.09
0.55
<5
640
0.
0.
<5
1,100
13 0.21
38 0.61
<5
740
0.51
0.45
<5
* Table A-2 identifies the source of analytical data for each used oil sample. Table A-3 provides codes
for each sample number which describes the specific generating source of used oil and the end-use.
T Numbers in parentheses represent EPA sample numbers for used oil samples obtained as part of their
1983 sampling program.
A-S:
-------
ANALYTICAL DATA FOR USED OIL SAMPLES
Sample Number*t
697(295) 698(296) 699(298)
Flash Point (*F)
Merals
Aiusir.um
Arsenic
Barium
Beryllium
Cadmium
Chromium
Cobalt
Copper
Iron
Lead
Magnesium
Manganese
Molybdenum
Nickel
Selenium
Silicon
Silver
Sodium
Tin
Titanium
Vanadium
Zinc
180
39
••*
130
<0
8
10
0
410
810
1,500
210
22
—
6
—
—
-
100
—
-
23
1,800
166
88
-------
TABLE A-l (continued)
ANALYTICAL DATA FOR USED OIL SAMPLES
Flash Point (°F)
Metals
Aluminum
Arsenic
Barium
Beryllium
Cadmium
Chromium
Cobalt
Copper
Iron
Lead
Magnesium
Manganese
Molybdenum
Nickel
Selenium
Silicon
Silver
Sodium
Tin
Titanium
Vanadium
Zinc
Volatile Organics
Dichlorodifludromethane
Trichlorofluoromethane
Trichlorotrifluoroethane
1,1,1-Trichloroethane
Trichloroethylene
Tetrachloroethylene
Phenol
Benzene
Toluer.e
Ethyl Bentene
Xylenes
Methvlene Chloride
Sample Number*t
705_(316) 706(319) 707(145) 708(171)709(172) 710(173) 711(175) 712(176)
148 164
14
<5
38
<0.2
1.3
3.3
<0.5
64
150
1,100
310
7.2
16
<5
53
<0.2
8.8
36
<0.5
50
140
920
220
6.6
150
<5
280
<0.2
<0.5
5.2
1.1
38
1,600
330
120
12
<1
120
110
230
3,500
270
1.20Q
1.1
2.4 -
180
340
<0.2 0.22 0.39
730 670 270
<8
<8
<8
<8
36
89
450
83
PNAS
Naphthalene
Penanthr ene /Anthracene
Pyrene
Benzo (a) anthracene
Benzo(a)pyrene
Alkylberizene (C-
Alkylnaphthalene
Phosphorus
Chlorine, wt 2
Sulfur, wt X
PCBs
)
720
0.12
0.43
<5
590
0.04
0.30
<5
530
0.74 0.17
0.59
0.07 0.05
0.58
0.16 0.14
<0.06
* Table A-2 identifies the source of analytical data for each used oil sample. Table A-3 provides codes
for each sample number which describes the specific generating source of used oil and the end-use.
+ Numbers in parentheses represent EPA sample numbers for used oil samples obtained as part of their
1983 sampling program.
A-S-.
\
-------
TABLE A-l (continued)
ANALYTICAL DATA FOR USED OIL SAMPLES
Sample Number*t
Flash Point (°F)
Metals
Aluminum
Arsenic
Barium
Beryllium
Cadmium
Chromium
Cobalt
Copper
Iron
Lead
Magnesium
Manganest
Molybdenum
Nickel
Selenium
Silicon
Silver
Sodium
Tin
Titanium
Vanadium
Zinc
Volatile Organics
t ichlorodifluoromethane
Tnchlo re fluorome thane
Trichlorotrifluoroethane
1,1,1-Trichloroethane
Trichloroethylene
Tetrachloroethylene
Phenol
Benzene
Toluene
Echyl Benzene
Xylenes
Methylene Chloride
713(178)714(179)715(183)716(184)717(185)718(186)719(192)720(194)
>200 - 13-V 132
26
<5
6.5
<0.2
<0.5
15
3.5
40
200
31
45
2.3
340
<5
13
<0.2
<0.5
10
7.0
29
750
49
4.9
4.4
33
<5
30
<0.2
1.5
21
1.1
120
1.400
600
180
27
12
<5
25
<0.2
0.94
2.5
0.84
52
110
340
75
3.8
4.5
61
15
7.0 -
15
390
1.0 -
42
0.46 0.25 -
110 64
<12 2,300
<12 1,400
<12 1.300
1.2 <0.2
1,300 320
210
<26
<26
38
89
940
340
1.100
<26
580
590
840
<26
190
630
790
260
1.700
PNAs
Naphthalene
Penanthrene/Anthracene
Pyrene
Benzo(a)anthracene
Benzo(a)pyrene
Alkylbenzene (C H,,,)
» 1 t l 1_*_1 1 ? T^
Alkylnaphthalene
Phosphorus
Chlorine, wt %
Sulfur, wt %
PCB<;
tC12H12>
310 290
0.16 0.57
0.40 <0.06 -
<5 24
0.07
0.19
<0.06
0.12
0.15
720
0.12
0.22
<5
440
0.09
0.26 -
<5 580
0.11
* Table A-2 identifies the source of analytical data for each used oil sample. Table A-3 provides codes
for each sample number which describes the specific generating source of used oil and the end-use.
t Numbers in parentheses represent EPA sample numbers for used oil samples obtained as part of their
1983 sampling program.
A-85
0276
-------
TABLE A-l (continued)
ANALYTICAL DATA FOR USED OIL SAMPLES
Sample Nuober*t
Flash Point (*F)
Metals
Aluminum
Arsenic
Barium
Beryllium
Cadmium
Chromium
Cobalt
Copper
Iron
Lead
Magnesium
Manganese
Molybdenum
Nickel
Selenium
Silicon
Silver
Sodium
Tin
Titanium
Vanadium
Zinc
221(195) 722(197)
>200 >200
140 16
<5 <5
31
<0.
<0.
6.
1.
29
390
210
42
4.
-
2.
-
-
-
190
-
-
1.
110
2
5
5
2
9
1
2
33
<0.2
0.66
4.7
0.5
22
170
530
42
6.5
-
0.88
-
-
-
76
-
-
<0.2
310
223U90) 224UW) 2j-5U°L) 726UQ3
140 130 >200 >200
65 7.2 58 11
<5 <5 200
12 20
<5 <5
35
<0.
1.
4.
<0.
28
160
1,300
390
11
-
1.
-
-
-
110
-
-
1.
960
2
6
1
5
3
3
- 27
<0.2
1.2
5
<0.5
33
170
930
130
5.6
-
1.3
-
-
-
110
-
-
0.2
660
Volatile Organics
Dichlorod ifluoromethane
Trichlorofluoromethane
Trichlorotrifluoroethane
1,1,1-Trichloroethane
Trichloroethylene
Tetrachloroethylene
Phenol
Benzene
Toluene
Ethyl Benzene
Xylenes
Methylene Chloride
60
180
52
<14
410
98
640
<14
7,200
22
66
63
450
170
1,700
<12
2,000
2,800
1,900
340
3,100
1,800
2,900
<16
1,600
1,100
340
360
2,800
590
1,600
1,000
140
35
22
<4
90
12
85
<4
190
170
800
370
1,200
900
380
830
1,400
PSAS
Naphthalene
Penar.threne /Anthracene
Pyrene
Benzo (a) anthracene
Benzo(a)pyrene
Alkylbenzene CC-H.
Alkylnaphthalene
,)
Phosphorus
Chlorine, vt X
Sulfur , wt 7.
PCBs
340
0.
0.
<5
37
30
390
0.20
0.19
<5
440
0.30
0.44
<5
640
0.15
0.48
<5
380
0.
0.
<5
2.100
06
36
0.06
0.47
<5
890
0.07
0.58
<5
680
0,
0.
<5
23
49
* Table A-2 identifies the source of analytical data for each used oil sample. Table A-3 provides codes
for each sample number which describes the specific generating source of used oil and the end-use.
t Numbers in parentheses represent EPA sample numbers for used oil samples obtained as part of their
1983 sampling program.
A-86
-------
TABLE A-l (continued)
ANALYTICAL DATA FOR USED OIL SAMPLES
Sample Number*t
Flash Point (°F)
Metals
Aluminun
Arsenic
Barium
Beryllium
Cadmium
Chromium
Cobalt
Copper
Iron
Lead
Magnesium
Manganese
Molybdtnum
Nickel
Selenium
Silicon
Silver
Sodium
Tin
Titanium
Vanadiun
Zinc
VoJatile Oreanics
Dichlorodifluoromethane
Trichlorofluoromethane
Trichlorotrifluoroethane
1,1,1-Trichloroethane
Trichloroethylene
Tetrachlcroethylene
Pher.cl
Benzene
Toluene
Ethyl Benzene
Xylenes
Methylene Chloride
729(224) 730(225)^731(232) 7j2(244) 733(251) 734(252) 735(253) 736(254)
>200 >200 126 >200 128 - - >200
480'
6.0
42
<0.2
<0.5
1.3
0.54
12
240
52
29
3.9
1.2
360
0.3
190
2.5
<5
6.3
<0.2
<0.5
0.64
<0.5
7.4
32
170
21
1.3
13
<5
28
<0.2
0.95
2.3
<0.5
55
130
700 1
36
3.7
12
<5
110
<0.2
0.98
4.2
0.61
31
190
.900
260
11
8.7
<5
10
<0.2
0.6
1.7
<0.5
22
150
440
76
4.2
15
<5
27
<0.2
1.6
5.4
1.1
63
200
840
220
12
<1
32
1.1
<1
1.6
26 100
49 100
<0.2 0.57 <0.2 <0.2 <0.2
280 440 820 340 760
<13
200
240
76
4,500
340
850
9,500
<17
<17
<17
1,100
1.600
260
2,200
<17
<8
<8
<8
<8
120
86
440
<8
<8
<8
<8
<8
<8
<8
120
<8
<7
<7
<7
<7
<7
<7
<7
<7
PNAs
Naphthalene
Penanthrene/Anthracene
Pyrene
Benzo(a)anthracene
Benzo(a)pyrene
Alkylbenzene (C.H..,)
Alkylnaphthalene tc.,Hno)
Phosphorus " A
Chlorir.e, wi %
Sulfur, wt 7.
PCBs
320
0.
0.
<5
1,500
,02 0.14
54 0.59
<5
790
0.08
0.45
<5
330
0.07
0.37
<5
690
0.10
0.51
<5
730
<0.01 <0.01 2.
0.
- <5
34
75
* Table A-2 identifies the source of analytical data for each used oil sample. Table A-3 provides codes
for each sarr.ple number which describes the specific generating source of used oil and the end-use.
T Na-bers in parentheses represent EPA sample numbers for used oil samples obtained as part of their
1983 sampling program.
A-87
0277
-------
TABLE A-l (continued)
ANALYTICAL DATA FOR USED OIL SAMPLES
Sample Number*!
737(270)738
Flash Point (°F)
Metals
Aluminum
Arsenic
Barium
Beryllium
Cadmium
Chromium
Cobalt
Copper
Iron
Lead
Magnesium
Manganese
Molybdenum
Nickel
Selenium
Silicon
Silver
Sodium
Tin
Titanium
Vanadium
Zinc
Volatile Organics
Dichlorodifluoromethane
Trichlorof luoromethane
Trichlorotrifluoroe thane
1,1,1-Trichloroethane
Trichloroethylene
Tetrachloroethylene
Phenol
Benzene
Toluene
Ethyl Benzene
Xylenes
Methylene Chloride
>147
2.8
<5
26
<0.2
0.56
0.67
<0.5
24
57
130
12
1.7
-
<1
-
-
-
5.8
-
-
<0.2
400
-
-
-
8,400
18
110
_
100
310
100
700 -
570
>i47
-
28
72
-
<8
<5
-
77
145
935
-
-
-
<5
-
-
-
-
-
-
<5
918
-
-
-
<100
<100
<100
-
-
-
-
-
-
739
>147
-
19
92
-
<8
<5
-
65
106
665
-
-
-
<5
-
-
-
-
-
-
<5
920
-
-
-
<100
<100
<100
-
-
-
-
-
-
740 741
>147
-
10 28
23 55
-
<8 <8
<5 <5
-
30 68
49 138
<6 1,050
-
-
- -
<5 <5
-
-
-
-
-
- -
<5 <5
287 867
- -
-
- -
- <100
- <100
- <100
-
-
-
-
-
- -
741
>147
-
28
58
-
8
<5
-
75
138
1,061
-
-
-
<5
-
-
-
-
-
-
<5
877
-
-
-
<100
<100
<100
-
-
-
-
-
-
743
>147
-
18
44
-
<8
<5
-
82
115
559
-
-
-
<5
-
-
-
-
-
-
<5
694
-
-
-
100
<100
<100
-
-
-
-
-
-
744
>147
-
<5
7
-
<8
<5
-
17
90
17
-
-
—
<5
-
-
-
-
-
-
15
51
-
-
-
<100
<100
<100
-
-
-
-
-
-
PNAs
Naphthalene
Penanthrene/Anthracene
Pyrene
Benzo(a)anthracene
Benzo(a)pyrene
Alkylbenzene (CgH._)
Alkylnaphthalene tc.JL.-)
Phosphorus
Chlorine, wt Z
Sulfur, wt Z
PCBs
—
500
0.75
0.73
<5
— — — — — — —
__ — _---
0.07 0.05 0.11 0.09 0.10 0.06 0.05
_______
* Table A-2 identifies the source of analytical data for each used oil sample. Table A-3 provides codes
for each sample number which describes the specific generating source of used oil and the end-use.
t Numbers in parentheses represent EPA sample numbers for used oil samples obtained as part of their
1983 sampling program.
A-88
-------
ANALYTICAL DATA FOR USED OIL SAMPLES
Sample Number*
Flash Point (°F)
Metals
Aluminum
Arsenic
Barium
Beryllium
Cadmium
Chromium
Cobalt
Copper
Iron
Lead
Magnesium
Manganese
Molybdenum
Nickel
Selenium
Silicon
Silver
Sodium
Tin
Titanium
Vanadium
Zinc
Volatile Organics
Dichlorodifluoromethane
Trichlorofluoromethane
Trichlorotrifluoroethane
1,1,1-Trichloroethane
Trichloroethylene
Tetrachloroethylene
Phenol
Benzene
Toluene
Ethyl Benzene
Xylenes
Methylene Chloride
745
>147
<5
<5
746
>147
7
162
<5
<5
15
747
>147
<5
39
748
>147
23
76
749
>147
38
67
750 751
>147 >147
<8
<5
29
133
<6
<8
7
85
1,340
563
<8
<5
6,230
470
<6
<8
<5
48
106
1,010
<8
<5
96
202
1.460
<5
<5
<5
<5
6
10
<8
<5
15
69
209
<5
11
228
<8
324
73
1.130
2,210
12
752
>147
18
52
<8
<5
41
129
761
<5 <5
989 1,850
<100
<100
<100
<5
716
500
<100
<100
<5
788
<100
<100
<100
<5
95
600
<100
<100
34
385
14
477
200 300
<100 <100
<100 <100
PNAs
Naphthalene
Penanthrene/Anthracene
Pyrene
Benzo(a)anthracene
Benzo(a)pyrene
Alkylbenzene (CgH,,)
Aiiwlnaphthalene tC^-H,,)
Phosphorus
Chlorine, wt Z
Sulfur, wt %
PCBs
<0.01 0.09
0.12
0.14
0.05
<20
0.17 0.14
<2 <10
0.13
<2
* Table A-2 identifies the source of analytical data for each used oil sample. Table A-3 provides codes
for each sample number which describes the specific generating source of used oil and the end-use.
A-89
0278
-------
TABLE A-l (continued)
ANALYTICAL DATA FOR USED OIL SAMPLES
Flash Point C'F)
Metals
Aluminum
Arsenic
Barium
Beryllium
Cadmium
Chromium
Cobalt
Copper
Iron
Lead
Magnesium
Manganese
Molybdenum
Nickel
Selenium
Silicon
Silver
Sodiun
Tin
Titanium
Vanadium
Zinc
753
>147
-
20
52
-
<8
<5
-
55
151
939
-
-
-
<5
-
-
-
-
-
-
10
648
754
>147
-
<5
<5
-
<8
<5
—
<5
<5
<5
-
-
-
<5
-
-
-
-
-
-
<5
<5
755
>147
-
<5
14
-
<8
<5
-
18
124
<6
-
-
-
<5
-
-
-
-
-
-
<5
<5
Sample
756
>147
-
<5
17
-
<8
<5
-
50
929
466
—
-
—
<5
-
-
-
-
-
-
<5
652
Number*
757
>147
-
8
755
-
57
459
—
630
9,580
273
—
-
-
Ill
-
-
-
-
-
-
69
383
758
>147
-
15
126
-
<8
108
—
54
888
1.110
-
—
-
10
-
-
-
-
-
-
35
387
759
>147
-
19
95
-
<8
<5
-
48
161
1,460
-
-
-
<5
-
-
-
-
-
-
<5
876
760
>147
-
12
•' 35
-
<8
<5
-
27
25
<6
-
-
-
<5
-
-
-
-
-
-
<5
198
Volatile Organics
Dichlorodifluoromethane
Tnchlorofluoromethane
Trichlorotrifluoroethane
1,1,1-Trichloroethane
Trichloroethylene
Tetrachloroethylene
Phenol
Benzene
Toluene
Erhyi Benzene
Xylenes
Methylene Chloride
300
<100 <100
<100 <100
100
<100
<100
<100
<100
<100
100 <1QO
<100 <100
<100 <100
PNAs
Naphthalene
Penanthrene/Anthracene
Pyrene
Benzo(a)anthracene
Benzo(a)pyrene
Alkylbenzene (C.H..)
Alkylnaphthalenl tc,,H12)
Phosphorus
Chlorine, «t T.
Sultur, wt %
PCBs
0.17
<2
<0.01 0.20
0.23
<2
0.13
<2
0.15
0.08
0.04
* Table A-2 identifies the source of analytical data for each used oil sample. Table A-3 provides codes
for each sample number which describes the specific generating source of used oil and the end-use.
A-90
-------
ANALYTICAL DATA FOR USED OIL SAMPLES
Flash Point (°F)
Sample Number*
761
>147
762
>147
763
>147
764
>147
765
>147
766
>147
767
>147
768
>147
Metals
Aluminum
Arsenic
Barium
Beryllium
Cadmium
Chromium
Cobalt
Copper
Iron
Lead
Magnesium
Manganese
Molybdenum
Nickel
Selenium
Silicon
Silver
Sodium
Tin
Titanium
Vanadium
Zinc
8
51
<8
<5
41
186
792
19
49
<8
<5
31
97
588
<5
12
94
<8
10
45
415
714
11
40
108
<8
<5
37
56
<8
<5
53 45
179 176
1,510 1,530
<5
<5
<5
129
<8
12
35
1,010
8
17
<5
92
<8
5
25
1,840
<6
<5
<5
<5
<8
<5
<5
<5
<6
<5
18
531
8
414
46 <5 <5
555 1,020 901
136
16
56
21
<5
<5
Volatile Organics
IHchlorodifluorooethane
Trichlorofluoromethane
Trichlorotrifluoroethane
1,1,1-Trichloroethane
Trichloroethylene
Tetrachloroethylene
Phenol
Benzene
Toluene
Ethyl Benzene
Xyler.es
Methylene Chloride
<100 <100
<100 <100
300 <1QO
<100
<100
<100
<100 300
<100 <100
100 100
Alkylbenzene
Alkylnaphthalene tc
Phosphorus
Chlorine, wt %
Sulfur, vt Z
PCBs
0.16
0.06
0.10
0.11
0.10
0.72 0.28
<0.01
<5
* Table A-2 identifies the source of analytical data for each used oil sample. Table A-3 provides codes
for each sample number which describes the specific generating source of used oil and the end-use.
A-91
0279
-------
TABLE A-l (continued)
ANALYTICAL DATA FOR USED OIL SAMPLES
Sample Number*t
Flash Point (°F)
Metals
Aluminum
Arsenic
Barium
Beryllium
Cadmium
Chromium
Cobalt
Copper
Iron
Lead
Magnesium
Manganese
Molybdenum
Nickel
Selenium
Silicon
Silver
Sodium
Tin
Titanium
Vanadium
Zinc
Volatile Organics
Dichlorodifluoromethane
Trichlorofluoromethane
Trichlorotrifluoroethane
1,1,1-Trichloroethane
Trichloroethylene
Tetrachloroethylene
Phenol
Benzene
Toluene
Ethyl Benzene
Xylenes
Methylene Chloride
PNAs
Naphthalene
Penanthrene/Anthracene
Pyrene
Benz o(a)anthracene
Benzo(a)pyrene
769 770 771 772(333) 773(348) 774(354) 775(356) 776(1)
>147 >147 - >200 - - >200
-
65
91
-
<8
19
_
52
7,890
185
_
-
-
65
38
-
<8
<5
-
31
233
498
-
-
-
5
207
-
<8
30
-
57
2.940
440
-
-
<1
<5
5.2
<0.2
0.92
<0.5
<0.5
39
19
10
<0.5
<0.2
3.0
<5
4.1
<0.2
<0.5
0.86
<0.5
14
24
<5
7.4
0.52
6.6
<5
1.9
<0.2
<0.5
16
<0.5
1.7
120
<5
4.0
1.2
2.3
<5
0.78
<0.2
<0.5
3.8
<0.5
29
23
13
4.0
0.85
16
<5
4.3
,<0.2
<0.5
1.2
<0.5
3.3
89
<5
9.2
3.7
18
21
78
161
20
368
97
278
<100 200 200
<100 <100 <100
<100 <100 <100
6.8
<0.2
400
530
160
61
190
72
<0.2
4.9
3.6 130
<0.2
6.2
<0.2
4.4
2.1
16
<0.2
69
<16
<16
<16
38
230
150
1,100
<16
<2
<2
<2
<2
<2
<2
<2
<2
310
<4
2.5
<4
12
<4
<4
<4
Phosphorus
Chlorine, wt Z
Sulfur, wt X
PCBs
- - 500
0.51 0.09 0.14 o.ll
-
<10 2 <10 <5
24
0.13
0.33
<5
21
<0.01
0.29
4.9
0.03
0.44
69
0.13
0.27
<5
* Table A-2 identifies Che source of analytical data for each used oil sample. Table A-3 provides codes
for each sample number which describes the specific generating source of used oil and the end-use.
+ Numbers in parentheses represent EPA sample numbers for used oil samples obtained as part of their
1983 sampling program.
A-92
-------
TABLE A-l (continued)
ANALYTICAL DATA FOR USED OIL SAMPLES
Flash Point (°F)
Metals
Aluminum
Arsenic
Barium
Beryllium
Cadmium
Chromium
Cobalt
Copper
Iron
Lead
Magnesium
Manganese
Molybdenum
Nickel
Selenium
Silicon
Silver
Sodium
Tin
Titanium
Vanadium
Zinc
Volatile Organics
Dichlorodifluoromethane
Trichlorofluoromethane
Trichlorotrifluoroethane
1,1,1-Trichloroethane
Trichloroethylene
Tetrachloroethylene
Phenol
Benzene
Toluene
Ethyl Benzene
Xylenes
Methylene Chloride
PNAs
Naphthalene
Penanthrene/Anthracene
Pyrene
Benzo(a)anthracene
Benzo(a)pyrene
Sample Number* t
777 (2) 776 (3) 779 (4) 780 (5) 781 (6) 782 (10)283 (51)2M (52)
>200 >200 >200 >200 >200 >75 >200 >200
68
<5
2.4
<0.2
<0.5
3.4
<0.5
2.5
560
6.0
4.2
2.2
1.1
260
<5
3.2
<0.2
<0.5
690
<0.5
55
820
9.8
18
4.7
5.8
340
<5
1.9
<0.2
<0.5
560
<0.5
52
470
6.0
20
3.4
1.8
19
<5
4.6
<0.2
<0.5
5.2
<0.5
2.2
310
12
48
8.6
23
3.6
<5
76
<0.2
<0.5
0.8
<0.5
21
89
110
1.9
1.2
<1
100
<5
51
<0.2
<0.5
18
1.6
5.6
490
56
96
4.4
7.3
4.9
<5
240
<0.2
2.6
1.5
<0.5
0.96
38
<5
9.1
0.49
3.6
1.0
<5
56
.2
<0.5
<0.5
6.9
4.0
13
<5
0.72
0.21
<1
2.8 11
<0.2 <0.2
24 62
6.6 13
1.2 15
0.26 <0.2 <0.2
55 130
<4
<4
<4
<4
<4
<4
<4
<4
250
59
1.10Q
<4
19
<4
39
<4
17
<4
5.7
94
<4
<4
<4
<4
39
<4
<4
<4
19
<4
59
<4
<0.2
31
<2
<2
<2
<2
7.3
19
<2
<2
18
68
<7
8.2
<7
<7
<7
250
1,200
<7
<0,
17
<6
<6
<6
<6
16
<6
<6
<6
270 280
.2 <0.2
16
<3
<3
<3
<3
9
<3
<3
<3
Alkylbenzene (C-IL.)
Alkylnaphthalene tc.,H12)
Phosphorus
Chlorine, wt Z
Sulfur, wt Z
PCBs
-
120
0.10
0.41
<5
_
290
0.10
0.84
<5
-
300
0.21
0.81
<5
-
270
0.35
0.51
<5
-
140
0.22
0.44
<5
-. ->
_
130 6,700 2,700
0.05 0.04
1.30 0.20
<11 <5
0.44
1.02
<5
* Table A-2 identifies the source of analytical data for each used oil sample. Table A-3 provides codes
for each sample number which describes the specific generating source of used oil and the end-use.
t Numbers in parentheses represent EPA sample numbers for used oil samples obtained as part of their
1983 sampling program.
A-93
0280
-------
TABLE A-l (continued)
ANALYTICAL DATA FOR USED OIL SAMPLES
Flash Point (*F)
Metals
Aluminum
Arsenic
Barium
Beryllium
Cadmium
Chromium
Cobalt
Copper
Iron
Lead
Magnesium
Manganese
Molybdenum
Nickel
Selenium
Silicon
Silver
Sodium
Tin
Titanium
Vanadium
Zinc
Volatile Organics
Dichlorodifluoromethane
Trichlorofluoromethane
Trichloro trifluoroethane
1,1,1-Trichloroethane
Trichloroethylene
Tetrachloroethylene
Phenol
Benzene
Toluene
Ethyl Benzene
Xylenes
Methylene Chloride
PNAs
Naphthalene
Penanthrene/Anthracene
Pyrene
Benzo(a)anthracene
Benzo(a)pyrene
Sample Number* t
785. (62) 286 (63) 787_ (64) 788 (65) 789 (66) 790 (67) 791 (92) 792 (93)
>200 84 164 140 >200 158 >200 >200
36
<5
29
<0.2
1.1
9.1
<0.5
33
280
1.200
180
11
1.0
9.5
7.6
26
<0.2
1.1
2.7
1.1
30
120
490
94
6.2
1.1
14
<5
20
<0.2
1.3
4.3
<0.5
36
180
980
330
7.4
<1
5.1
<5
6.6
<0.2
0.93
<0.5
34
2.9
87
110
180
1.3
<1
14
<5
32
<0.2
1.4
5.2
<0.5
35
240
770
390
10
1.8
15
<5
58
<0.2
1.6
4.6
<0.5
72
240
1,100
300
9.0
1.5
<1
<5
<0.5
<0.2
<0.5
<0.5
<0.5
5.0
3.2
<5
<0.5
<0.2
<1.0
13
<5
4.2
<0.2
<0.5
<0.5
<0.5
<0.5
41
<5
1.0
1.1
<1
81 110
100
210 150
110
<1.0 1.2
<0.2 0.21 <0.2 <0.2 0.35 <0.2 <0.2 0.51
930 410 910 640 1,000 910 6.7 22
<4
7
<4
<4
270
<4
150
<4
290
46
320
<5
1,900
300
430
-1,200
190
80
67
230
1,300
580
530
11
37
20
13
_
1,700
260
410
18
160
95
20
24
1,000
110
270
<5
360
110
46
360
1,400
450
550
67
<2
<2
<2
<2
<2
<2
<2
<2
<5
<5
<5
<5
<5
<5
<5
<5
Alkylbetizene (C.E,,)
Alkylnaphthalene tc12H12)
Phosphorus
Chlorine, wt Z
Sulfur, wt %
PCBs
~"
920
0.07
0.54
<5
~
540
0.11
0.80
<5
"
820
0.09
0.56
<5
_
620
0.05
0.49
<5
~
920
0.21
0.62
<5
-
800 180 31
0.09 0.02 0.01
0.51 0.25 0.81
<5 <5 <5
* Table A-2 identifies the source of analytical data for each used oil sample. Table A-3 provides codes
for each sample number which describes the specific generating source of used oil and the end-use.
t Numbers in parentheses represent EPA sample numbers for used oil samples obtained as part of their
1983 sampling program.
A-94
-------
TABLE A-l (continued)
ANALYTICAL DATA FOR USED OIL SAMPLES
Sample Number*t
Flash Point (°F)
Metals
Aluminum
Arsenic
Barium
Beryllium
Cadmium
Chromium
Cobalt
Copper
Iron
Lead
Magnesium
Manganese
Molybdenum
Nickel
Selenium
Silicon
Silver
Sodium
-Tin
Titanium
Vanadium
Zinc
Volatile Organics
Dichlorodifluoromethane
Tr ichlorofluoromethane
Trichlorotrifluoroethane
1,1,1-Trichloroethane
Trichloroethylene
Tetrachloroethylene
Phenol
Benzene
Toluene
Ethyl Benzene
Xylenes
Methylene Chloride
PNAs
Naphthalene
Penanthrene/Anthracene
Pyrene
Benzo(a)anthracene
Benzo(a)pyrene
293 (94) 794fl22) 295J797) 796(.320) 227(326)
<80 >200 112 >200 >200 >200
799(.328) 800(329)
>200 >200
25
<5
18
<0.2
0.52
2.8
2. 4
38
96
180 1
9.9
2.0
1.0
14
<5
770
<0.2
1.9
6.4
1.7
25
250
,900
380
10
1.5
14
<5
130
<0.2
1.0
7.4
0.59
153
680
810
100
16
2.7
1.3
<5
<0.5
<0.2
<0.5
<0.5
<0.5
5.4
21
5.6
4.8
0.22
1.1
5.2
<5
13
<0.2
0.88
1.7
<0.5
28
130
390
110
5.2
1.8
2.3
<5
2.4
<0.2
<0.5
<0.5
<0.5
1.2
72
8.5
6.4
0.65
10
4.4
<5
14
<0.2
1.7
4.6
<0.5
16
85
460
110
3.1
2.9
13
<5
45
<0.2
1.6
3.1
1.4
89
150
790
160
5.2
1.2
5.2 42
91
12
150
19
120
400
<0.2 <0.2 0.36 0.53 3.7 46 8.7 0.45
130 1.000 500 18 790 6.0 390 380
12,000
6,100
21,000
<330
12,000
1,600
3,200
5,100
<7
<7
<7
190
940
440
960
- <7
<6
<6
72
80
370
130
600
<6
<15
<15
<15
38
290
<15
1,100
<15
140
320
60
100
73
520
93
83
100
1,200
160
340
140
60
<8
35
100
890
150
950
890
Alkylbenzene (CQH.,)
AlKylr.aphchalene \C H )
Phosphorus
Chlorine, wt Z
Sulfur, wt '/.
PCBs
-
-
510
0.
0.
<5
-
-
1,100
14 0.08
19 0.48
<5
-
-
660
0.37
0.44
<5
-
-
100
<0.01
0.18
<5
-
-
850
0.06
0.54
<5
-
-
26
0.27
0.72
<5
-
-
420
0.20
0.49
<5
-
-
510
0.07
0.38
<5
* Table A-2 identifies the source of analytical data for each used oil sample. Table A-3 provides codes
for each sample number which describes the specific generating source of used oil and the end-use.
t Numbers in parentheses represent EPA sample numbers for used oil samples obtained as part of their
1983 sampling program.
A-95
0281
-------
TABLE A-l (continued)
ANALYTICAL DATA FOR USED OIL SAMPLES
Flash Point (°F)
Metals
Aluminum
Arsenic
Barium
Beryllium
Cadmium
Chromium
Cobalt
Copper
Iron
Lead
Magnesium
Manganese
Molybdenum
Nickel
Selenium
Silicon
Silver
Sodium
Tin
Titanium
Vanadium
Zinc
Volatile Organics
Dichlorodifluoromethane
Trichlorofluoromethane
Trichlorotrifluoroethane
1,1.1-Trichloroethane
Trichloroethylene
Tecrachloroethylene
Phenol
Benzene
Toluene
Ethyl Benzene
Xylenes
Methylene Chloride
PSAs
Naphthalene
Penanthrene/Anthracene
Pyrene
Benzo(a)anthracene
Benzo(a)pyrene
Sample Number*!
801(335) 802(337) £03(338) 80^339) 805(340) 806(341) 807.(342) 808(
190
5.7
<5
48
<0.2
0.95
1.6
<0.5
59
160
1,100
77
5
194
2.2
<5
<0.5
<0.2
<0.5
<0.5
0.53
<0.5
7.9
<5
23
<0.2
140
10
<5
35
<0.2
1.2
5.1
1.6
40
220
660
89
3.5
>200
5.5
<5
11
<0.2
0.74
2.0
0.51
32
81
840
460
5.2
170
9.5
<5
25
<0.2
0.95
2.7
<0.5
46
120
870
170
5.5
86
7.3
<5
17
<0.2
<0.5
1.2
<0.5
21
170
360
24
1.9
164
11
<5
25
<0.2
0.89
2.7
<0.5
46
120
850
170
5.2
<75
7.4
f5
62
<0.2
0.84
2.1
<0.5
39
120
940
140
5.4
1.3
55
46
10
1.8
1.1
1.9
2.6
92 110 130 230
1.1
99
1.5
88
2.7 190 4.6 0.67 0.44 8.8 0.29 3.8
860 30 400 1.000 720 310 680 660
<16 1.900
<16 140
<16 1,000
<16 2,500
<16 9,900
<16 760
160 3,200
<16 100
<8
<8
<8
<8
120
88
590
<8
<4
<4
<4
63
190
" <4
390
<4
43
46
140
200
5,800
520
2,100
<16
<4
<4
<4
<4
63
45
200
<4
740
<14
60
290
1,900
330
1,600
<14
240
190
1,900
7,400
1,500
6,700
100
Alkylbenzene (CgH-,)
Alkylnaphthalene tc12H12>
Phosphorus
Chlorine, wt X
Sulfur, wt t
PCBs
:
780
0.08
0.46
<5
:
29
0.10
2.44
<5
:
590
0.08
0.71
<5
-
930
0.04
0.47
<5
:
720
0.09
0.46
<5
:
370
1.23
0.51
<5
-
640
0.13
0.83
<5
-
610
0.12
0.26
<5
* Table A-2 identifies the source of analytical data for each used oil sample. Table A-3 provides codes
for each sample number which describes the specific generating source of used oil and the end-use.
t Numbers in parentheses represent EPA sample numbers for used oil samples obtained as part of their
19S3 sampling prograr..
A-96
-------
TABLE A-l (continued)
ANALYTICAL DATA FOR USED OIL SAMPLES
Flash Point (°F)
Metals
Aluminum
Arsenic
Barium
Beryllium
Cadmium
Chromium
Cobalt
Copper
Iron
Lead
Magnesium
Manganese
Molybdenum
Nickel
Selenium
Silicon
Silver
Sodiur.
Tin
Titanium
Vanadium
Zinc
Volatile Organics
Dichlorodifluoromethane
Trichiorofluoromethane
Trichlorotrifluoroethane
1,1,1-Trichloroethane
Trichloroethylene
Tetrachloroethylene
Phenol
Benzene
loiuer.e
Ethyl Benzene
Xylenes
Methylene Chloride
PNAs
Naohthalene
Per.anthrene /Anthracene
Pyrene
Benzo(a)anthracene
Benzo(a)pyrene
Alkvlbenzene (CgH.,)
Alr.yir.apnthalene TC, ,H.,)
Sample Number* t
809 (344 )BlO(345-> 811(359) 812(360) 81389) 814(90) 815(91) 81&95)
94 <80 >200 >200 >200 >200 >200 136
7.9
<3
48
<0.2
0.87
2.2
<0.5
36
110
950
130
5.6
1.4
l.t
<5
52
<0.2
0.79
2.0
<0.5
35
100
850
150
5.3
1.2
17
<5
8.4
<0.2
<0.5
3.7
<0.5
6.1
100
9.4
9.8
0.52
1.5
2.3
<5
380
<0.2
1.5
0.94
0.68
5.3
18
<5 1
10
0.4
<1
17
<5
22
<0.2
1.0
5.2
<0.5
75
210
,200
220
6.7
<1
22
<5
33
<0.2
1.4
5.3
<0.5
28
250
470
390
9.6
1.3
6.4
<5
280
<0.2
<0.5
<0.5
<0.5
100
9.0
<5
510
0.38
<1
11
<5
32
<0.2
0.64
3.7
<0.5
26
120
490
86
3.5
1.7
130
140 3,800
300
98
170
24
460
2.8 2.9 <0.2 <0.2 <0.2 0.6 <0.2 2.4
630 590 17 13 750 890 910 280
1,600
240
530
640
9,200
440
1,900
390
870
480
870
320
11,000
1,100
2,200
-<15
<4
<4
<4
<4
<4
<4
<4
<4
1,200
<1
1.600
1
2
3
<1
<1
300
<4
20
180
770
260
350
<4
140
54
7.8
30
200
120
157
<4
<4
<4
<4
<4
<4
<4
<4
<4
310
110
430
150
1,100
520
540
<10
Phosphorus
Chlorine, vt X
Sulfur, wt %
PCBs
570
0.
0.
<5
13
27
540
0.16
0.39
<5
310
0
0
<5
6,700
.09 0.
.45 0.
<5
1,100
03 0.52
59 0.09
<5
680
0.40
0.53
<5
600
<0.01
0.41
<5
490
0.
0.
<5
18
53
* Table A-2 identifies the source of analytical data for each used oil sample. Table A-3 provides codes
for each sample Dumber which describes the specific generating source of used oil and the end-use.
+ Numbers in parentheses represent EPA sample numbers for used oil samples obtained as pert of their
19S3 sanpling program.
A-97
0282
-------
TABLE A-l (continued)
ANALYTICAL DATA FOR USED OIL SAMPLES
Flash Point (°F)
Metals
Aluminum
Arsenic
Barium
Beryllium
Cadmium
Chromiun
Cobalt
Copper
Iron
Lead
Magnesium
Manganese
Molybdenum
Nickel
Selenium
Silicon
Silver
Sodium
Tin
Titanium
Vanadium
Zinc
Volatile Organics
Dichlorodifluoromethane
Tnchlor of luorome thane
Trichlorotrifluoroethane
1,1,1-Trichloroethane
Trichloroethylene
Tetrachloroethylene
Phenol
Benzene
Toluer.e
Ethyl Benzene
Xylenes
Methylene Chloride
PNAs
Naphthalene
Penanthrene/Anthracene
Pyrene
Benzo(a)anthracene
Benzo(a)pyrene
Sample Number*t
817(96) 818(98) 819(99) 820(101) 821(102) 822(103) 823(214) 824(216)
200 134 >200 >200 96 >200 146 116
14
<5
32
<0.2
0.79
7.2
0.58
24
180
610
200
7.9
1.6
4.2
<5
51
<0.2
<0.5
2.6
<0.5
10
36
230
20
1.1
1.8
16
<5
33
<0.2
1.0
5.6
<0.5
28
140
740
140
6.8
1.3
5.0
<5
120
<0.2
5.8
1.9
<0.5
33
52
83
66
1.5
<1.0
44
<5
19
<0.2
<0.5
3.6
<0.5
21
190
190
7.8
1.3
1.1
16
<5
35
<0.2
1.2
3.8
<0.5
47
160
920
260
11
<1
7.0
<5
21
<0.2
0.68
9.6
10
35
140
99
12
5.3
2.0
3.4
<5,
3.0
<0.2
<0.5
1.9
1.2
6.8
52
9.8
5.9
1.3
15
130 170
26
16
3.5 110
5.5 23
2.0 0.23 0.88 <0.2 <0.2 <0.2 0.35 23
660 59 720 670 120 930 160 80
18
29
100
_
200
170
320
<8
5,600
200
3,500
230
3,000
720
,1,200
120
630
150
330
_
36
300
460
<17
3,500
30
380
19
230
270
520
<15
12,000
40
270
59
860
290
630
170
<17
<17
27
. 62
270
96
730
<19
9,100
11,000
5.100
<14
780
270
1,100
2,800
13,000
37,000
9.300
<17
9,100
10,000
12,000
1,200
Alkylbenzene (C.H., ,)
Alkylnaphthalene tC. _K. ,)
Phosphorus
Chlorine, vt Z
Sulfur, wt %
FCBs
-
800
0.05
0.66
<5
-
-
300 1.000
0.35
0.36
<5
0.18
0.66
<5
-
470
0.17
0.40
<5
-
300
0.21
0.44
<5
-
830
<0.01
0.47
<5
-
410
1.89
0.50
<5
-
62
2.58
0.7Z
<5
* Table A-2 identifies the source of analytical data for each used oil sample. Table A-3 provides codes
for each sample number which describes the specific generating source of used oil and the end-use.
t Numbers in parentheses represent EPA sample numbers for used oil samples obtained as part of their
1983 sampling program.
A-98
-------
TABLE A-l (continued)
ANALYTICAL DATA FOR USED OIL SAMPLES
Sample Number*t
Flash Point (°F)
Metals
Aluminum
Arsenic
Barium
Beryllium
Cadmium
Chromium
Cobalt
Copper
Iron
Lead
Magnesium
Manganese
Molybdenum
Nickel
Selenium
Silicon
Silver
Sodium
Tin
Titanium
Vanadium
Zinc
Volatile Organics
Dichlorodifluoronethane
Trichlorofluoromethane
Tnchlorotriiluoroethane
1,1,1-Trichloroethane
Trichloroethylene
Tetrachloroethylene
Phenol
Benzene
Toluene
Ethyl Benzene
Xylenes
Methylene Chloride
PNAs
Naphthalene
Penanthrene/Anthracene
Pyrene
Benzo(a)anthracene
Benzo(a)pyrene
825(217) 826(226) 827(227) 828(234) 8,29(235) 830(236) 831(237) 832(
116
2.7
<5
19
<0.2
<0.5
7.7
5.7
9.6
120
46
16
4.8
>200
2.2
<5
95
<0.2
<0.5
<0.5
<0.5
<0.5
45
6.1
4.4
1.5
-
1.9
<5
93
<0.2
<0.5
<0.5
<0.5
<0.5
42
11
4.0
1.5
<85
31
6.6
0.86
<0.2
2.8
52
9.3
69
72
51 2
1.2
4.0
>200
5.5
<5
0.76
<0.2
0.51
<0.5
<0.5
610
33
.000
<0.5
<0.2
>200
19
<5
35
<0.2
<0.5
<0.5
<0.5
8.5
4.5
87
9.2
1.5
-
31
<5
<0.5
<0.2
5.9
23
16
68
100
55
1.3
3.5
154
1
<5
"94
<0.2
<0.5
<0.5
<0.5
9.8
5.8
19
30
2.5
4.0
53
11
8.8
3.3
5.0
2.6
2.1
7.2
3.0
0.45 0.56 0.61 0.26 <0.2 <0.2 <0.2 <0.2
120 6.6 7.9 520 88 39 580 220
3.100 <16
24,000 <16
20,000 2,400
5,900 5,700
7,000 1,400
8,000 -590
1,700 51
<14 12,000
<14 3,100
1,300 1,200
1,800 55,000
<14 31,000
660 57,000
<14 9,300
70
<2 4,700
-------
ANALYTICAL DATA FOR USED OIL SAMPLES
Flash Point CD
Mecals
Aluminum
Arsenic
Barium
Beryllium
Cadmium
Chromium
Cobalt
Copper
Iron
Lead
Magnesium
Manganese
Molybdenum
Nickel
Selenium
Silicon
Silver
Sodium
Tin
Titanium
Vanadium
Zinc
Volatile Organics
Dichlorodifluoromethane
Trichlorofluoromethane
Tricolorotrifluoroethane
1,1,1-Trichloroethane
Trichlgroethylene
Tetrachloroethylene
Phenol
Benzene
Toluene
Ethyl Benzene
Xylenes
Methylene Chloride
PNAs
Naphthalene
Penanthrene/Anthracene
Pyrene
Ber.zo (a) anthracene
Benzo(a)pyrene
Sample Number*!
833(240)834(275)835(276)836(278)837(279)838(331) 839(332)
150
>200 >200
<1
<5
90
<0.2
0.56
<0.5
<0.5
9.8
6.7
16
25
2.5
<1
590
<5
7.8
<0.21
<0.5
2.2
0.68
1,4
130
44
1.6
0.42
<1
770
<5
14
<0.2
<0.5
1.5
<0.5
4.0
270
330
2.3
0.4
<1
760
<5
14
<0.2
<0.5
1.5
<0.5
3.6
220
290
1.3
<0.2
<1
910
<5
24
<0.2
<0.5
2.1
<0.5
6.0
170
220
3.6
0.53
<1
16
<5
120
<0.2
0.7
10
0.8
20
110
59
16
2.0
40
410
<5
5.0
<0.2
<0.5
2.0
<0.5
2.0
240
7.3
6.2
3.0
1.1
2.3 5.7 2.4 1.7
3.3 5.9
3.2
<0.2 <0.2 <0.2 <0.2 <0.2 <0.2 <0.2
200 3.7 2.3 1.9 6.0 120 30
<14 <16 <15 <16 <4
<14 <16 <15 <16 <4
<14 <16 <15 <16 <4
<14 <16 <15 <16 <4
<14 <16 <15 <16 <4
<14 <16 <15 <16 <4
540 <16 <15 <16 37
<14 <16 <15 <16 <4
Alkylbenzene (CgH..)
Alkylnaphthalene tc.-lL-)
Phosphorus
Chlorine, wt X
Sulfur, wt 2
PCBs
350
8.67
0.60
<5
280
0.07
0.49
<5
220
<0.01
0.39
<5
110
<0.01
0.45
<5
91
<0.01
0.06
<5
280
0.06
-
<5
240
0.15
-
<5
* Table A-2 identifies the source of analytical data for each used oil sample. Table A-3 provides codes
for each sample number which describes the specific generating source of used oil and the end-use.
T Numbers in parentheses represent EPA sample numbers for used oil samples obtained as part of their
1983 sampling program.
A-100
-------
TABLE A-l (continued)
ANALYTICAL DATA TOR USED OIL SAMPLES
Sample Number*
840 841 842 843 844 845 846 847
Flash Point (°F) ________
Metals
Aluminum ----____
Arsenic ________
Barium 82 96.2 88 81.3 88.3 89.5 79.4 85
Beryllium ________
Cadmium 2.7 3 5 4.7 4.8 2 4.2 2.7
Chromium 9.8 12 16.3 8 14.5 16.8 12.8 6.3
Cobalt ________
Copper ________
Iron ________
Lead 93.8 257.3 118.3 86 129.7 21.8 183.6 87.5
Magnesium ________
Manganese ________
Molybdenum ________
Nickel ________
Selenium ________
Silicon ________
Silver ________
Sodium ________
Tin ________
Titanium ________
Vanadium ________
Zinc 1,125 965 900 1,100 1,133 1,020 1,166 923
Volatile Organics
Dichlorodifluoromethane ________
Trichlorofluoromethane ________
Trichlorotrifluoroethane ________
1,1,1-Trichloroethane ________
Trichloroethylene ________
Tetrachloroethylene ________
Phenol ________
Benzene - - - - - --
Toluene ________
Ethyl Benzene ________
Xylenes ________
Methylene Chloride - " -
PNAs
naphthalene ________
Penanthrene/Anthracene - - - - - - - • -
Pyrene ________
Benzo(a)anthracene ________
Benzo(a)pyrene ________
Alkylbenzene (C H ,) ________
Alkylnaphthalene tC1_H1_) ________
Phosphorus i- i- ________
Chlorine, wtZ ________
Sulfur, wt % ________
PCBs ________
* Table A-2 identifies the source of analytical data for each used oil sample. Table A-3 provides codes
for each sample number which describes the specific generating source of used oil and the end-use.
A-101
0283
-------
TABLE A-l (continued)
ANALYTICAL DATA FOR USED OIL SAMPLES
Sample Number*
86.3
6.5
12.8
87
4.0
11.0
77.5
0.3
5.8
91.5
0.9
9.5
75.0
2.0
11.5
103.1
0.7
8.1
102.3
1.3
7.7
T6.5
0.5
5.0
848 849 850 851 852 853 854 855
Flash Point (°F) ________
Metals
Aluminum — ~ ~ •* ~ — _ •*
Arsenic
Barium
Beryllium
Cadmium
Chromium
Cobalt _________
Copper ________
Iron ________
Lead 161.3 77.8 120 85.1 115 95.8 53 69.0
Magnesium ________
Manganese __.-__«_
Molybdenum ________
Nickel ________
Selenium ________
Silicon ________
Silver ________
Sodium ________
Tin ________
Titanium ________
Vanadium ________
Zinc 950 1.160 1,758 906.3 1,050 951.4 936.7 1,125
Volatile Organics
Dichlorodifluorotnethane ________
Trichlorofluoromethane ________
Trichlorotrifluoroethane ________
1,1,1-Trichloroethane ________
Trichloroethylene ________
Tetrachloroethylene -___-_•_
Phenol ________
Benzene ________
Toluene _----___
Ethyl Benzene __-_---_
Xylenes --- - - - _
Methylene Chloride ________
PNAs
Naphthalene ________
Penantnrene/Anthracene ________
Pyrene ________
Benzo(a)anthracene ________
Benzo(a)pyrene ________
Alkylbenzene (CqH12) ________
Alkylnaphthalene tc,-H ,) -
Phosphorus ^ ________
Chlorine, wtX _____•___
Sulfur, wtl ________
PCBs ________
* Table A-2 identifies the source of analytical data for each used oil sample. Table A-3 provides codes
for each sample number which describes the specific generating source of used oil and the end-use.
A-102
-------
TABLE A-l (continued)
ANALYTICAL DATA FOR USED OIL SAMPLES
Flash Point (°F)
Metals
Aluminum
Arsenic
Barium
Beryllium
Cadmium
Chromium
Cobalt
Copper
Iron
Lead
Magnesium
Manganese
Molybdenum
Nickel
Selenium
Silicon
Silver
Sodium
Tin
Titanium
Vanadium
Zinc
856
94.8
1.1
7.7
91.3
Sample Number*
857
82.8
0.2
5.8
51.0
858
83.5
1.3
10.0
82.0
859
80.6
0.2
5.8
860
95.6
0.7
6.0
87.3 103.3
861
90.0
1.7
7.7
84.3
862
65.0
3.0
10.0
863
74.8
2.4
7.9
90.0 309.3
1,251 1,522
917.5 1,541 1,157
842 1,050 1,177
Volatile Organics
Dichlorodifluorome thane
Trie hi orofluorome thane
Trichlorotrif luoroethane
1 ,1,1-Trichloroethane
Trichloroethyleixe
Tetrachloroethylene
Phenol
Benzene
Toluene
Ethyl Benzene
Xylenes
Methylene Chloride
PNAs
Naphthalene
Penanthrene /Anthracene
Pyrene
Benzo(a)anthracene
Benzo(a)pyrene
Alkylbenzene (ClL )
Alkylnaphthalen
Phosphorus
Chlorine, wt Z
Sulfur, vt 7.
PCBs
. -,H1-)
* Table A-2 identifies the source of analytical data for each used oil sample. Table A-3 provides codes
for each sample number which describes the specific generating source of used oil and the end-use.
A-103
0285
-------
TABLE A-l (continued)
ANALYTICAL DATA TOR USED OIL SAMPLES
Flash Point (°f)
Metals
Aluminum
Arsenic
Barium
Beryllium
Cadmium
Chromium
Cobalt
Copper
Iron
Lead
Magnesium
Manganese
Molybdenum
Nickel
Selenium
Silicon
Silver
Sodium
Tin
Titanium
Vanadium
Zinc
Volatile Organics
Dithlorodifluoromethane
Trichlorofluoromethane
Trichlorotrifluoroethane
1,1,1-Trichloroethane
Trichloroethylene
Tetrachloroethylene
Phenol
Benzene
Toluene
Ethyl Benzene
Xylenes
Methylene Chloride
PNAs
Naphthalene
Penanthrene/Anthracene
Pyrene
Benzo(a)anthracene
Benzo(a)pyrene
Alkylbenzene (CqH,,)
Alkylnaphthalene tc.,H ,)
Phosphorus
Chlorine, wt Z
Sulfur, wt 2
PCBs
Sample Sunbcr*
864
865
866
867
868
869
870
871
82.5
1.1
8.7
68.4
0.6
12.0
102.5 1,323.3
84.3
0.5
5.0
70.2
76.1
2.0
8.0
56.3
94.3
1.4
6.0
77.4
85.1
1.4
10.4
69.8
1.3
15.3
78.9 133.4
76.0
5.8
97.6
915 1,291
872 1,082.8 901 1,600 1,644
916
* Table A-2 identifies the source of analytical data for each used oil sample. Table A-3 provides codes
for each sample number which describes the specific generating source of used oil and the end-use.
A-104
-------
TABLE A-l (continued)
ANALYTICAL DATA FOR USED OIL SAMPLES
"lash Point (•?)
Metals
Aluminum
Arsenic
Barium
Beryllium
Cadmium
Chromium
Cobalt
Copper
Iron
Lead
Magnesium
Manganese
Molybdenum
Nickel
Selenium
Silicon
Silver
Sodium
Tin
Titanium
Vanadium
Zinc
Volatile Organics
);ichlorodifluorome thane
Trichlorofluoromethane
Trichlorotrifluoroethane
1,1,1-Trichloroethane
Trichloroethylene
Tetrachloroethylene
Phenol
Benzene
Toluene
Ethyl Benzene
Xylenes
Methylene Chloride
PSAs
Naphthalene
Penanthrene/Anthracene
Pyrene
Benz o (a) ant hracene
Benzo(a)pyrene
Alkylbenzene (CqH17)
Alkylnaphthalene tc. -1L.)
Phosphorus •"•
Chlorine, wt %
Sulfur, wt Z
PCBs
Sample Number*
872
873
874
875
876
877
878
879
79.0
0.3
25.3
77.9
1.0
18.6
70.0
0.6
32.6
87.3
0.3
31.0
70.0
0.7
25.0
67.7
0.3
26.7
68.0 30.7
0.9
21.3
1.0
19.3
12.242 18,063 18,500 12.400 20.333 17.8 16,637 17,037
915
980 1,214 1.077 1,050 1.067 1,169 1.112.5
* Table A-2 identifies the source of analytical data for each used oil sample. Table A-3 provides codes
for each sample number which describes the specific generating source of used oil and the end-use.
A-105
0286
-------
TABLE A-l (concinued)
ANALYTICAL DATA FOR USED OIL SAMPLES
Sample Number*
Flash Point (*F)
Metals
Aluminum
Arsenic
Barium
Beryllium
Cadmium
Chromium
Cobalt
Copper
Iron
Lead
Magnesium
Manganese
Molybdenum
Nickel
Selenium
Silicon
Silver
Sodium
Tin
Titanium
Vanadium
Zinc
Volatile Organics
Dichlorodif luorome thane
Tr ichlorof luor ometnane
Trichlorotrif luoroe thane
1,1,1-Trichl or oe thane
Trichloroethylene
Tetrachloroethylene
Phenol
Benzene
Toluene
Ethyl Benzene
Xylenes
Methylene Chloride
880
>147
-
<5
<7
-
<7
<5
-
<5
11
6
-
-
<5
<5
-
-
-
-
-
-
<5
254
-
-
-'
2,300
<100
<100
-
-
-
-
-
-
881
142
-
9
<7
-
< 7
6
—
18
113
202
-
-
<5
<5
-
-
-
-
-
-
<5
197
-
-
-
9,200
<100
<100
-
-
.
-
-
-
882
M47
-
<5
10
-
<7
14
-
43
48
16
-
-
<5
<5
-
-
-
-
-
-
<5
168
-
-
-
600
<100
<100
-
-
-
-
-
-
883
>147
-
<5
18
-
147
-
18
31
-
<7
9
_
38
184
1,000
-
-
<6
<5
-
-
-
-
-
-
<5
952
-
-
-
4,700
<100
300
-
-
-
-
-
-
885
133
_
13
19
-
9
9
_
38
148
507
-
-
<6
<5
-
_
_
-
_
_
<5
380
_
_
_
10,000
.4.200
3,000
_
-
_
-
-
-
886
142
_
<5
90
_
<5
52
»
69
783
725
-
-
19
<5
-
.
_
-
_
_
19
597
_
_
_
2,700
1,900
1,900
v
_
_
-
-
-
887
>147
_
22
10
_
<5
<5
»
30
107
1,240
-
.
<6
<5
—
_
_
_
_
_
<5
300
_
_
_
6,000
1,400
11,000
_
_
_
-
-
-
PNAs
Naphthalene
Penanthrene /Anthracene
Pyrene
Benzo (a) anthracene
Benzo(a)pyrene
Alkylbenzene (Cg
Alkylnaphthalene
Phosphorus
Chlorine, vt Z
Sulfur, vl I
PCBs
0.19 0.99 0.08 3.23 0.36
1.95
<50
0.32 3.26
* Table A-2 identifies the source of analytical data for each used oil sample. Table A-3 provides codes
for each sample number which describes the specific generating source of used oil and the end-use.
A-106
-------
ANALYTICAL DATA FOR USED OIL SAMPLES
Sample Number*
Flash Point CF)
Metals
Aluminum
Arsenic
Barium
Beryllium
Cadmium
Chromium
Cobalt
Copper
Iron
* Lead
Magnesium
Manganese
Molybdenum
Nickel
Selenium
Silicon
Silver
Sodium
Tin
Titanium
Vanadium
Zinc
Volatile Organics
Dichlorodifluorome thane
Trichlorofluoromethane
Trichlorotrifluoroe thane
1,1, 1-Trichloroe thane
Trichloroethylene
Tetrachloroethylene
Phenol
Benzene
Toluene
Ethvl Benzene
Xvlerxes
Methylene Chloride
888
108
-
18
17
-
<5
<5
-
60
102
1,200
-
-
<6
<5
-
-
-
-
-
-
<5
366
-
-
-
5,200
5,700
24,000
-
-
-
-
-
-
889 890
>U7
- -
<5 <5
99 39
-
9 <5
126 31
-
89 16
671 337
915 28
-
— -
8 <6
<5 <5
-
-
-
-
-
- -
7 <5
214 50
-
-
- -
30,000
800
4,500
- —
-
-
-
-
-
891
>147
-
<5
<9
-
<5
<5
-
<5
5
<5
-
-
<6
<5
-
-
-
-
-
-
<5
<5
-
-
-
<100
<100
<100
—
-
-
-
-
-
892
)147
-
<5
284
-
<5
37
-
103
613
141
-
-
<6
<5
-
-
-
-
-
-
6
148
-
-
-
900
<100
<100
-
-
-
-
-
-
893 894
>147 >147
- -
<5 <5
42 91
_ •;
<5 <5
<5 7
-
6 6
87 2.570
5 57
-
- -
<6 <6
<5 15
-
-
-
-
-
- -
<5 22
8 224
-
-
- -
200
-
- • -
— -
-
-
-
-
895
>147
-
26
40
-
<10
8
-
53
173
815
-
-
5
<5
-
-
-
-
-
-
<5
962
-
-
-
<100
<100
<100
-
-
-
-
-
-
PSAs
Naphthalene __-__-__
Penanthrene/Anthracene __-__-__
Pyrene ________
Benzo(a)anthracene ________
Benzo(a)pyrene ________
Alkylbenzene (C.H..) __-_-___
Alkylnaphthalene tc.-H,,) __----_-
Phosphorus --------
Chlorine, wt % *-72 1.22 0.35 <0.01 0.34 0.26 0.29 0.04
Sulfur, wt% __-__-__
PCBs <10 • <50 - <1 <50 - <10 <10
* Table A-2 identifies the source of analytical data for each used oil sample. Table A-3 provides codes
for each sample number which describes the specific generating source of used oil and the end-use.
A-107
0287
-------
TABLE A-l (continued)
ANALYTICAL DATA FOR USED OIL SAMPLES
Sample Number*
896 897
Flash Point (°T> >147 >147
Metals
Aluminum
Arsenic 19 9
Barium 30 40
Beryllium
Cadmium <10 <10
Chromium 25 118
Cobalt
Copper 34 63
Iron 166 282
Lead 636 725
Magnesium
Manganese
Molybdenum <5 6
Nickel <5 <5
Selenium
Silicon
Silver
Sodium
Tin
Titanium
Vanadium <5 <5
Zinc 923 569
Volatile Organics
Dichlorodifluoromethane
Trichlorofluoromethane
Trichlorotrifluoroethane
1.1,1-Trichloroethane 200 <100
Trichloroethylene <100 <100
Tetrachloroethylene 600 20,000
Phenol
Benzene -
Toiuer.e
Ethyl Benzene
Xylenes -
Methylene Chloride
PSAs
Naphthalene -
P enar.Lhrene/Anthracene
Pyrene
Benzo(a)anthracene
Benzo(a)pyrene - -
Alkylber.zene (CQH.,)
Alkylnaphthalene tc. ,H .)
Phosphorus -
Chlorine, wt 7. 0.11 3.69
Sulfur, wt % - -
PCBs <10 <10
* Table A-2 identifies the source of analytical data for each used oil sample. Table A-3 provides codes
for each sample number which describes the specific generating source of used oil and the end-use.
A-108
-------
TABLE A-l (continued)
ANALYTICAL DATA FOR USED OIL SAMPLES
Sample Number*
Flash Point (°F)
Metals
Aluminum
Arsenic
Barium
Beryllium
Cadmium
Chromium
Cobalt
Copper
Iron
Lead
Magnesium
Manganese
Molybdenum
Nickel
Selenium
Silicon
Silver
Sodium
Tin
Titanium
Vanadium
Zinc
Volatile Organics
Dichlorodifluoromethane
Trichlorofluoromethane
Trichlorotrifluoroethane
1,1,1-Trichloroethane
Tn;r.loroethylene
letraenioroethylene
Phenol
Benzene
Toluene
Ethyl Benzene
Xylenes
Metr.vlene Chloride
PNAs
Naphthalene
Penanthrene/Anthracene
• Pyrene
Benz o(a)anthracene
B«nzo(a)pyrene
898
>147
<5
<7
<7
9
44
270
39
<5
27
<5
86
<100
<100
<100
899
>147
<5
31
<7
<5
156
11
15
16
<5
36
<100
<100
<100
Alkylbenzene (C.Ii
Alkylnaphthalene
Phosphorus
Chlorine, wt Z
Sulfur, wt X
?CBs
900
>147
<5
82
<7
13
37
221
72
<5
11
901
>147
<5
11
<7
<5
21
232
20
<5
7
<5
566
1,600
200
3,800
<5
54
<100
600
600
902
>147
<5
<7
<7
<5
6
33
11
<5
<5
<5
<5
200
<100
<100
903
>147
<5
10
<7
11
30
316
41
6
33
<5
76
2,400
200
1,300
904
>147
<5
29
<7
10
34
306
30
7
26
<5
183
905
>147
<5
<7
<7
7
46
73
<5
<5
<5
<5
<5
1,600 900
200 <100
7,700 200
1.34
<50
0.05
1.38
<50
0.72
<50
1.20
<50
1.14
<50
1.40 0.61
<50 <10
* Table A-2 identifies the source of analytical data for each used oil sample. Table A-3 provides codes
for each sample number which describes the specific generating source of used oil and Che end-use.
A-109
0288
-------
TABLE A-l (continued)
ANALYTICAL DATA FOR USED OIL SAMPLES
Sample Number*
Flash Point (°F)
Metals
Aluminum
Arsenic
Barium
Beryllium
Cadmium
Chromium
Cobalt
Copper
Iron
Lead
Magnesium
Manganese
Molybdenum
Nickel
Selenium
Silicon
Silver
Sodium
Tin
Ticaniun
Vanadium
Zinc
906
TCT
_
<5
18
-
<7
16
-
6
482
13
-
-
12
21
-
-
-
-
-
'
<5
47
907
-
<5
55
-
<7
91
-
71
1.100
18
-
-
315
47
-
-
-
-
-
-
<5
106
908
>147
-
<5
10
-
<7
12
-
• 25
392
40
-
-
7
23
-
-
-
-
-
-
<5
116
322
>147
_
<5
38
—
<7
8
-
16
212
39
-
-
<5
8
-
-
-
-
-
.
<5
249
*
«,
<5
41
-
<7
62
-
55
321
<5
-
-
58
15
-
-
-
-
-
-
<5
34
911
w
<5
33
_
<7
181
_
201
28
<5
-
-
31
13
.
-
-
-
-
_
<5
86
912
^
<5
1.100
_
27
440
_
1,140
12.300
893
-
-
987
1.840
-
_
-
-
_
_
450
8.610
913
—
<5
116
.
<7
209
_
76
3.250
57
-
-
45
100
_
_
_
_
_
_
19
1.600
Volatile Organics
Dichlorodifluoromethane
Trichloroiluoromethane
Trichlorotrifluoroethane
1,1,1-Trichloroethane
Trichloroethylene
Tetrachloroethylene
Phenol
Benzene
Toluene
Ethyl Benzene
Xylenes
Methylene Chloride
PNAs
Naphthalene
Penanthrene/Anthracene
Pyrene
Benzo(a)anthracene
Benzo(a)pyrene
Alkylbenzene (C-H.,)
Alkylnaphthalene tc.-Hj-)
Phosphorus
200"
400
1,000
5,100
100
400
1,500
400
6.900
<100
<100
<100
<100
<100
<100
500
200
2.100
Chlorine, wt X
Sulfur, wt I
PCBs
0.64 0.29 1.07
-
<50 - <50
1.53 0.09
-
<50 <10
0.10 0.20 0.65
-
<10 - <50
* Table A-2 identifies the source of analytical data for each used oil sample. Table A-3 provides codes
for each sample number which describes the specific generating source of used oil and the end-use.
A-110
-------
TABLE A-l (concinued)
ANALYTICAL DATA FOR USED OIL SAMPLES
Sample Number*
Flash Point (CF)
Metals
Aluminum
Arsenic
Barium
Beryllium
Cadmium
Chromium
Cobalt
Copper
Iron
Lead
Magnesium
Manganese
Molybdenum
Nickel
Selenium
Silicon
Silver
Sodium
Tin
Titanium
Vanadium
Zinc
Volatile Organics
Dichlorodifluoromethane
Trichlorof luorotne thane
Trichlorotrifluoroethane
1,1,1-Trichloroethane
Trichloroethylene
Tetrachloroethylene
Phenol
Toluene
Ethyl Benzene
Xvlenes
Methylene Chloride
PN'As
Napnthaier.e
Penant hrene /Ant hracene
Pyrene
Benzo(a)anthracene
Benzo(a)pyrene
Alkylbenzene (CgH,,)
Alkylnaphthalene ^i2H\2^
Phosphorus
Chlorine, wt %
Sulfur, wt 7.
?C5s
914
>147
<5
547
18
363
237
15,000
1,180
1,490
721
117
8.120
915
>147
<5
205
<7
253
>147
9
552
8
571
149 1,160
1,020 4,930
33 317
96
96
387
528
917
>147
<5
70
<7
31
11
152
30
<5
7
36
588
300
200
1,000
113
3,550
<5
152
1,000
800
300
0.46
0.15
0.20
0.43
918
>147
<5
458
<7
125
66
3,150
64
30
322
919
>147
<5
61
<7
24
<5
307
19
<5
7
384
650
<5
122
<100 <100
<100 1,000
<100 1,000
0.15
1.01
<50
920
>147
<5
12
<7
42
26
<5
18
<5
<5
13
9_21
>147
5
22
<5
10
22
549
118
<6
6
<5
392
1.000
200
3,000
0.13
0.45
* Table A-2 identifies the source of analytical data for each used oil sample. Table A-3 provides codes
for each sample number which describes the specific generating source of used oil and the end-use.
A-lll
0289
-------
TABLE A-l (continued)
ANALYTICAL DATA FOR USED OIL SAMPLES
Sample Dumber*
Flash Point (°F)
Metals
Aluminum
Arsenic
Barium
Beryllium
Cadmium
Chromiun
Cobalt
Copper
Iron
Lead
Magnesium
Manganese
Molybdenum
Nickel
Selenium
Silicon
Silver
Sodium
Tin
Titanium
Vanadium
Zinc
Volatile Organics
Dichlorodifluorome thane
Trichlorof luorotne thane
Tr ichlorotr if luoroe thane
1,1, 1-Trichloroethane
Trichloroethylene
Tetrachloroethylene
Phenol
Benzene
Toluene
Icrr. I Ber.zene
Xylenes
Methylene Chloride
922
>147
-
21
29
-
<5
8
-
20
170
502
-
-
<6
<5
-
-
-
-
-
-
<5
593
-
-
-
200
800
200
-
-
-
-
-
-
923
>147
-
<5
13
-
<5
7
-
42
110
11
-
—
<6
<5
-
-
-
-
-
-
<5
50
-
-
-
<100
<100
<100
-
-
-
-
-
-
924
>147
-
<5
28
-
<5
11
-
26
597
104
-
-
<6
9
-
-
-
-
-
-
<5
333
-
-
-
800
400
300
_
-
-
-
-
-
925
>147
-
<5
292
-
33
511
—
100
3.260
114
-
—
12
48
-
-
-
-
-
-
164
188
-
-
-
<100
<100
<100
_
-
-
-
-
-
926
>147
_
<5
76
_
7
84
_
34
1.080
10
-
-
<6
17
-
-
.
.
.
.
41
51
_
-
-
-
-
-
_
-
_
-
-
-
927
>147
_
<5
79
<5
107
_
363
1.150
163
-
-
7
10
.
-
_
_
_•
_
28
203
_
-
_
<100
200
<100
_
_
_
-
-
-
928
>147
_
<2
32
<5
28
_
29
502
<5
-
-
<6
<5
-
-
«
-
_
_
10
34
_
-
_
<100
<100
300
_
_
_
-
-
-
929
>147
^
4
26
<5
<5
_
<5
690
86
-
_
<6
47
_
-
_
_
_
_
<5
368
„
_
—
<100
<100
200
_
.
—
-
-
-
PSAs
Naphthalene
Penanthrene/Anthracene
Pyrer.e
Benzo(a)anthracene
Benzo(a)pyrene
Alkylbenzene (CgH^.)
Alkylnaphtr.slene tc.^H.,)
Phosphorus
Chlorine, wt X
Sulfur, wt %
PCBs
---_-___
" • " ^ —• -f •• ^
0.26 0.54 0.32 0.08 0.03 0.15 0.08 0.19
---_-___
* Table A-2 identifies the source of analytical data for each used oil sample. Table A-3 provides codes
for each sample number which describes the specific generating source of used oil and the end-use.
A-112
-------
TABLE A-l (continued)
ANALYTICAL DATA FOR USED OIL SAMPLES
Sample Number*
Flash Point (°F)
930
97
931
>147
932
61
933
>U7
934
97
935
>147
936
68
937
>147
Metals
Aluminum
Arsenic
Barium
Beryllium
Cadmium
Chromium
Cobalt
Copper
Iron
Lead
Magnesium
Manganese
Molybdenum
Nickel
Selenium
Silicon
Silver
Sodiun
Tin
Titanium
Vanadium
Zinc
Volatile Organics
Dichlorodifluorome thane
Trichlorofluorome thane
Trichlorotrifluoroethane
1,1, 1-Trichloroethane
Trichloroethylene
Tetrachloroethylene
Phenol
Benzene
Toluene
Ethyl Benzene
Xylenes
Methylene Chloride
PNAs
Naphthalene
Penan threr.e /Anthracene
Pyrene
Benzo (a ) anthracene
Benzo(a)pyrene
6
30
<5
124
264
1,100
240
<6
19
<5
233
<100
<100
200
Alkylbenzene
Alkylnaphthalene
Phosphorus
Chlorine, wt Z
Sulfur, wt "
PCBs
(C-H,0
0)
0.22
<2
75
7
<5
9
425
10
<6
<5
27
39
0.05
4
9
<5
<5
16
572
115
<6
10
<5
136
300
<100
1.500
0.35
<2
26
<5
<5
<6
<5
6
47
<100
<100
<100
0.02
6
31
<5
50
8 86
176 1.030
<5 350
<6
5
7
172
4,400
2.200
4.800
<5
91
<5
25
57
416
21
<6
<5
<5
379
9
106
19
51
74
60
600
500
800
373
518
<5
251
<5
6
105 58
8.330 728
404 35
<6
<5
7
220
<100 4,400
<100 <100
900 <100
L.32
<50
0.21
0.65
<50
* Table A-2 identifies the source of analytical data for each used oil sample. Table A-3 provides codes
for each sample number which describes the specific generating source of used oil and the end-use.
A-113
0290
-------
TABLE A-l ^continued;
ANALYTICAL DATA FOR USED OIL SAMPLES
Sample Number*
Flash Point (°F)
Metals
Aluminum
Arsenic
Barium
Beryllium
Cadmium
Chromium
Cobalt
Copper
Iron
Lead
Magnesium
Manganese
Molybdenum
Nickel
Selenium
Silicon
Silver
Sodium
Tin
Titanium
Vanadium
Zinc
Volatile Organics
Dichlorodifluoromethane
Trichlorofluoromethane
Trichlorotrif luoroe thane
1,1,1-Trichloroethane
Trichloroethylene
Tetrachloroethylene
Phenol
Benzene
Toluene
Ethvl Benzene
Xyier.es
Methylene Chloride
938
>147
-
<5
622
-
<5
42
-
167
1,220
52
-
-
<6
<5
-
-
-
-
-
-
27
252
-
-
-
5.400
<100
<100
-
-
-
-
-
-
939
>147
-
<5
718
-
<5
12
-
52
1.030
26
-
-
<6
<5
-
-
-
-
-
-
14
235
-
-
-
300
<100
<100
-
-
-
-
-
-
940
>147
-
<5
66
-
<5
<5
-
17
96
<5
-
-
<6
<5
-
-
-
-
-
-
<5
17
-
-
-
-
-
-
—
-
-
-
-
-
941
>147
-
<5
200
-
<5
8
-
75
252
24
-
-
<6
<5
-
-
-
-
-
-
<5
99
—
-
-
1.400
<100
<100
—
-
-
-
-
-
942
>147
-
<5
168
-
<5
10
-
6
201
10
-
-
<6
<5
-
-
-
-
-
-
<5
52
-
-
-
5,500
200
<100
•
-
-
-
-
—
943
>147
-
<5
74
-
<5
<5
-
17
114
<5
-
-
<6
<5
-
-
-
-
-
-
<5
9
-
-
-
-
-
-
~
-
—
—
—
—
944
>147
-
<5
159
- "
<5
12
-
159
374
32
-
-
<6
<5
-
-
-
-
-
-
11
187
—
-
-
<100
<100
<100
•
—
~
~
-
—
945
>147
-
<5
212
-
<5
15
-
124
434
25
-
-
<6
<5
-
-
-
-
-
-
<5
170
-
-
-
3,800
<100
<100
*
""
—
—
—
*
PKAs
Naphthalene
Penanthrene/Anthracene
Pyrene
Benzo(a)anthracene
Benzo(a)pyrene
Alkylbenzene (CgHj_)
Alkylnaphthalene TC,,H1,)
Phosphorus
Chlorine, wt Z
Sulfur, wt Z
PCBs
0.50
-
<50
0.10 0.17
— -
<20
0.50
-
<50
1.05 0.19
- *
<50
0.04
••
<5
0.81
— *
<50
* Table A-2 identifies Che source of analytical data for each used oil sample. Table A-3 provides codes
for each sample number which describes the specific generating source of used oil and the end-use.
A-114
-------
TABLE A-l (continued)
ANALYTICAL DATA FOR USED OIL SAMPLES
Sample Number*
946 947
Flash Point (8F) -
Metals
Aluminum - -
Arsenic <5 <5
Barium 524 171
Beryllium
Cadmium <5 <5
Chromium 36 11
Cobalt
Copper 210 84
Iron 2.990 338
Lead 44 26
Magnesium
Manganese
Molybdenum
Phosphorus
Chlorine, wt X 0.27 0.34
Sulfur, wt % -
PCBs - <50
* Table A-2 identifies the source of analytical data for each used oil sample. Table A-3 provides codes
for each sample number which describes the specific generating source of used oil and the end-use.
A-115
0291
-------
TABLE A-l (.continues,)
ANALYTICAL DATA FOR USED OIL SAMPLES
Sample Number*
Flash Point (°F)
Metals
Aluminum
Arsenic
Barium
Beryllium
Cadmium
Chromium
Cobalt
Copper
Iron
Lead
Magnesium
Manganese
Molybdenum
Nickel
Selenium
Silicon
Silver
Sodium
Tin
Titanium
Vanadium
Zinc
Volatile Organics
Dichlorodif luoromethane
Trichlorof luoromethane
Tr ichlorotr if luoroe thane
1,1, 1-Trichloroethane
Trichloroethylene
Tetrachloroethylene
Phenol
Benzene
Toluene
Et-.yl 3er.zeT\e
Xylenes
Methylene Chloride
948
129
-
<5
122
-
<7
42
-
82
2.560
1,160
-
-
<5
20
-
-
-
-
-
-
26
1,160
-
-
-
5,000
200
600
-
-
-
-
-
- ,
9_49
117
-
12
16
-
<7
72
-
181
1.260
321
-
-
<5
«5
-
-
-
-
-
-
6
83
-
-
-
200
<100
1,100
-
-
-
-
-
-
950
>147
-
<5
217
-
<7
32
-
21
1,580
1,760
-
-
12
14
-
-
-
-
-
-
37
1.680
-
-
-
400
<100
200
-
-
-
-
-
-
951
>147
-
<5
249
-
<7
45
-
172
2,630
191
-
-
<5
13
-
-
-
-
-
-
29
255
-
-
-
<100
<100
<100
-
-
-
-
-
-
952
>147
-
147
.
8
9
-
<7
332
_
612
2,040
106
-
-
7
17
.
.
-
-
-
-
<5
122
_
-
.
<100
<100
<100
-
-
_
-
-
-
954
>147
_
6
<7
-
<7
47
_
448
1,490
102
-
-
<5
10
_
.
_
-
-
_
<5
56
_
-
-
<100
<100
<100
-
-
_
.
-
-
955
>147
_
16
48
.
<7
241
_
550
4,690
595
-
-
9
32
_
_
_
-
_
.
9
512
• _
-
-
<100
<100
<100
_
-
_
-
-
-
PNAs
Naphthalene
Penan threne/Anthracene
Pyrer.e
Benzo(a) anthracene
Benzo(a)pyrene
Alkylbenzene (C.H..)
Alkylnaphthalene tC.,)
Phosphorus
Chlorine, wt Z
Sulfur, wt 2
FCBs
_
0.56 0.40 0.39 0.10
_ _ _ _
<10 <10 <5 <5
-
0.07
-
32
-
<0.01
-
11
-
<0.01
-
7
-
0.04
-
'5
* Table A-2 identifies the source of analytical data for each used oil sample. Table A-3 provides codes
for each sample number which describes the specific generating source of used oil and the end-use.
A-116
-------
ANALYTICAL DATA FOR USET) OIL SAMPLES
Sample Number*
Flash Point (cf)
Mecals
Aluminum
Arsenic
Barium
Beryllium
Cadnuun
Chromium
Cobalt
Copper
Iron
Lead
Magnesium
Manganese
Molybdenum
Nickel
Selenium
Silicon
Silver
Sodium
Tin
Titaniun
Vanadium
Zinc
Volatile Organics
Dichlorodif luor one thane
Trichlorofluoromethane
Trichl orotr if luoroe thane
1,1, 1-Irichloroethane
Trichloroethylene
Tetrachloroethylene
Phenol
Benzene
Toluene
Ethvl Benzene
Xyler.e;
Methylene Chloride
956
>147
_
10
1.070
-
<7
87
-
600
8,570
388
-
-
12
40
-
-
-
-
-
-
<5
440
-
-
-
<100
<100
<100
-
-
-
-
-
-
957
>147
-
7
1,000
-
<7
65
-
369
971
209
-
-
<5
11
-
-
-
-
-
-
<5
249
-
-
-
<100
<100
<100
-
-
-
-
-
-
958
>147
-
20
708
-
<7
18
-
129
2,410
785
-
-
<5
13
-
-
-
-
-
-
11
678
-
-
-
200
<100
<100
-
-
-
-
-
-
959
>147
_
9
22
-
<7
9
-
275
6.780
267
-
-
8
35
-
-
-
-
-
-
7
233
-
-
-
<100
<100
<100
-
-
-
-
-
-
960
>147
_
15
27
-
<7
119
-
300
1.550
537
-
-
<5
10
-
-
-
-
-
-
<5
446
-
-
-
<100
<100
<100
-
-
-
-
-
-
961
>147
_
11
36
-
<7
35
-
359
18,600
129
-
-
13
48
-
-
-
-
-
-
18
162
-
-
-
<100
<100
<100
-
-
-
-
-
-
962
>147
_
6
26
-
147
_
7
48
-
<7
153
-
442
2.660
122
-
-
<5
21
-
-
-
-
-
-
<5
102
—
-
-
<100
<100
<100
-
-
-
-
-
-
PNAs
Naphtnaiene
Penanthrene/Anthracene
Pyrene
Benzo(a)anthracene
Benzo(a)pyrene
Alkylbenzene (C.H )
Alkylnaphthalene tc12H12>
Phosphorus
Chlorine, wt %
Sulfur, wt Z
PCBs
0.04
-
5
0.04
-
6
0.16
—
<5
0.02
-
6
0.03
-
2
<0.01
-
2
0.03
-
3
0.01
-
4
* Table A-2 identifies the source of analytical data for each used oil sample. Table A-3 provides codes
for each sample number which describes the specific generating source of used oil and the end-use.
A-117
0292
-------
TABLE A-l (continued)
ANALYTICAL DATA FOR USED OIL SAMPLES
Flash Point (°F)
Metals
Aluminum
Arsenic
Barium
Beryllium
Cadmium
Chromium
Cobalt
Copper
Iron
Lead
Magnesium
Manganese
Molybdenum
Nickel
Selenium
Silicon
Silver
Sodium
Tin
Titanium
Vanadium
Zinc
Volatile Organics
Dichlorodifluoromethane
Trichlorofluoromethane
Trichlorotrifluoroethane
1,1,1-Trichloroethane
Trichloroethylene
Tetrachloroethylene
Phenol
Benzene
Toluene
Ethyl Benzene
Xylenes
Methylene Chloride
PNAs
Naphthalene
Penanthrene/Anthracene
Pyrene
Benzo(a)anthracene
Benzo(a)pyrene
Alkylbenzene (CgH..)
Alkylnaphthalene tc.-H.,)
Phosphorus
Chlorine, vt Z
Sulfur, ut Z
PCBs
964
84
<5
23
94
125
276
69
<5
<5
965
115
<5
178
39
2.730
720
15
7
966
>147
<5
105
<5
1,050
322
18
5
Sample Number*
967
>147
<5
32
8
26
189
273
<5
<5
968
93
14
107
16
51
796
476
8
<5
969
>147
<5
285
25
32
2,800
607
8
12
970
111
8
520
<10
27
37
21.100
563
25
72
971
97
<5
8
<5
38
43
<5
<5
<5
117
161
1.070
4,400 <100
<100 <100
300 <100
20
421
<100
<100
<100
7
495
2.500
<100
700
21
991
6.100
«100
<100
224
797
238
659
300 30.000
26.000 <100
200 200
<5
21
<100
<100
1.600
0.15
<50
0.22
0.19
0.29
1.31
<50
2.69
<20
2.94
<100
0.09
* Table A-2 identifies the source of analytical data for each used oil sample. Table A-3 provides codes
for each sample number which describes the specific generating source of used oil and the end-use.
A-118
-------
TABLE A-l (continued)
ANALYTICAL DATA FOR USED OIL SAMPLES
Sample Number*
Flash Point (°F)
Metals
Aluminum
Arsenic
Barium
Beryllium
Cadmium
Chromium
Cobalt
Copper
Iron
Lead
Magnesium
Manganese
Molybdenum
Nickel
Selenium
Silicon
Silver
Sodium
Tin
Titanium
Vanadium
Zinc
Volatile Organics
Dichlorodifluorome thane
Trichlorofluorome thane
Trichloro tr if luoroe thane
1,1, 1-Tr ichloroethane
Trichloroethylene
Tetrachloroethylene
Phenol
Benzene
Toluene
Ethyl Benzene
Xylenes
Methylene Chloride
972
>147
-
12
235
-
<10
18
-
<5
5,330
342
-
-
5
12
-
-
-
-
-
-
287
431
-
-
-
500
<100
200
-
-
-
-
-
-
9,73
>147
-
<5
106
-
<10
8
-
9
2,860
286
-
-
29
<5
-
-
-
-
-
-
78
795
-
-
-
400
<100
1,000
-
-
-
-
_
-
974
>147
-
23
70
-
<10
11
-
37
283
<5
-
-
<5
<5
-
-'
-
-
-
-
<5
773
-
-
-
500
<100
300
-
-
-
-
-
-
975
>126
-
<5
10
-
<10
<5
-
44
25
<5
-
-
<5
<5
-
-
-
-
-
-
<5
33
-
-
-
200
<100
<100
-
-
-
-
-
-
976
>147
-
<5
30
-
<10
<5
-
7
1,100
8
-
—
8
9
-
-
-
-
-
-
<5
14
-
-
-
1,600
<100
300
-
-
-
-
-
-
977
>147
-
<5
20
-
<10
22
-
199
717
9
-
-
9
<5
-
-
-
-
-
—
<5
165
-
-
-
700
<100
900
-
-
-
-
-
-
978
>147
-
<$,
10
-
<10
8
-
7
1,060
17
-
—
IV
<5
-
-
-
-
-
-
<5
36
-
-
-
<100
<100
1,400
-
-
-
-
-
-
979
>147
—
<5
10
-
<10
<5
—
9
550
<5
-
—
<5
<5
-
-
-
-
-
-
<5
<5
-
-
-
-
-
-
-
-
-
-
-
-
PNAs
Naphthalene
Penanthrene/Anthracene
Pyrene
Benzo(a)anthracene
Benzo(a)pyrene
Airiylbenzene (CgK..,)
Alkylnaphthalene t£H)
Phosphorus
Chlorine , wt %
Sulfur, wt I
PCBs
1.58
-
<50
0.42
-
<20
0.14
-
6
0.73 0.96
-
<1 <20
1.10
-
<20
1.01
-
<20
0.18
-
* Table A-2 identifies the source of analytical data for each used oil sample. Table A-3 provides codes
for each sample number which describes the specific generating source of used oil and the end-use.
A-119
0293
-------
TABLE A-l (continued.)
ANALYTICAL DATA FOR USED OIL SAMPLES
Sample Number*
Flash Point (°F)
Metals
Aluminum
Arsenic
Barium
Beryllium
Cadmium
Chromium
Cobalt
Copper
Iron
Lead
Magnesium
Manganese
Molybdenum
Nickel
Selenium
Silicon
Silver
Sodium
Tin
Titanium
Vanadium
Zinc
Volatile Organics
Dichlorodifluorome thane
Trichlorofluoromethane
T r ichl orotr if luoroe thane
1,1, 1-Trichloroethane
Trichloroethylene
Tetrachloroe thy lent
Phenol
Benzene
Toluene
E;h_. i Berizer.e
Xylenes
Methylene Chloride
980 981
>147 >147
- -
<5 <5
<10 20
-
<;o 147
_
<5
<10
-
<10
<5
-
<5
<5
6
-
-
<5
U7
-
8
30
-
<10
18
-
28
834
327
-
-
13
8
-
-
-
-
-
-
<5
267
-
-
-
800
<100
800
-
-
-
-
.
-
984
>U7
_
9
20
-
<10
<5
-
41
202
518
-
-
<5
147 >147
_ „
<5 <5
30 <10
— — • >
<10 <10
<5 <5
_ _
6 <5
29 12
<5 12
-
-
<5 <5
<5 <5
-
-
_ •
_
-
_
<5 <5
17 330
-
.
-
1,200
<100
<100
- -
-
-
-
-
-
987
>147
_
21
<10
^
<10
8
_
12
222
747
-
-
<5
<5
_
-
_
_
_
_
<5
166
-
_
-
<100
<100
<100
_
-
-
-
-
-
PSAs
Naphthalene
Penanthrene/ Anthracene
Pyrer.e
Benzo(a)anthracene
Benzo(a)pyrene
Alkylbenzene (CgH..)
Alkvlnaohthalene TCH,,)
Phosphorus
Chlorine
Sulfur,
PCBs
, wt Z
wt 7.
0.04 <0.01 0.07
_
<1 - 44
0.73 0.66
-
<20 <10
0.09 0.16 0.05
_
<1 39
* Table A-2 identifies the source of analytical data for each used oil sample. Table A-3 provides codes
for each sample number which describes the specific generating source of used oil and the end-use.
A-l 20
-------
ANALYTICAL DATA FOR USED OIL SAMPLES
Sample Number*
Flash Point (°F)
Metals
Aluminum
Arsenic
Barium
Beryllium
Cadmium
Chromium
Cobalt
Copper
Iron
Lead
Magnesium
Manganese
Molybdenum
Nickel
Selenium
Silicon
Silver
Sodium
Tin
Titaniura
Vanadium
Zinc
Volatile Organics
D ..chlorodif luoromethane
Tricolor of luorome thane
Trichlorotrif luoroe thane
1, 1,1-Tnchloroethane
Trichloroethylene
Tecracr.loroethylene
Phenol
Benzene
Toluene
Ethyl Benzene
988
>147
-
<5
<10
-
<10
<5
-
<5
326
6
-
-
<5
<5
-
-
-
-
-
-
6
15
-
-
-
<100
<100
<100
-
-
-
-
989 990
>147 >147
- -
13 <5
80 30
-
<10 <10
431 168
- -
54 34
3,430 557
827 9
-
- -
<5 <5
8 6
-
-
-
-
-
- -
<5 8
263 273
-
-
-
1,000
5,400
6,100
-
-
-
-
991
>147
-
<5
10
-
<10
26
-
71
467
59
-
-
<5
<5
-
-
-
-
-
-
<5
23
-
-
-
400
<100
200
-
-
-
-
992
>147
-
<5
10
-
<10
10
-
229
415
58
-
-
<5
<5
-
-
-
-
-
-
<5
186
-
-
-
300
<100
400
-
-
-
-
993
>147
-
<5
50
-
<10
13
-
19
958
136
-
-
<5
<5
-
-
-
-
-
-
<5
211
-
-
-
1,100
<100
300
-
-
-
-
994
>147
-
<5
360
-
<10
104
_
218
6.020
259
-
-
12
24
-
-
-
-
-
-
36
650
-
-
-
300
<100
500
-
-
-
-
995
>147
-
<5
30
-
*10
42
_
220
1.900
86
-
—
<5
<5
-
-
-
-
-
-
<5
126
-
-
—
300
<100
400
-
-
-
-
Methyier.e Chloride
PN'As
Naphthalene
Penanthrene/Anthracene
Pvrene
3enzo(a;antnrace.r.e
Benzo(a)pyrene
Alkylbenzene (CgH,-)
Alkylnaphthalene tc.,H12)
Phosphorus
Chlorine, wt 7.
Sulfur, wt 2
PCBs
0.03
-
<5
0.62
-
53
0.14 0.39
- -
<50
0.78
—
<50
1.48
-
<50
1.66
-
<50
4.94
-
<50
* Table A-2 identifies the source of analytical data for each used oil sample. Table A-3 provides codes
aacn sample number which describes the specific generating source of used oil and the end-use.
A-121
0294
-------
TABLE A-l (concinuea;
ANALYTICAL DATA FOR USED OIL SAMPLES
Sample Number*
Flash Point (°F)
Metals
Aluminum
Arsenic
Barium
Beryllium
Cadmium
Chromium
Cobalt
Copper
Iron
Lead
Magnesium
Manganese
Molybdenum
Nickel
Selenium
Silicon
Silver
Sodvun
Tin
Titanium
Vanadium
Zinc
Volatile Organics
D ichlorod if luorome thane
Trichlorofluorome thane
Trichlorotrif luoroe thane
1 , 1 , 1-Trichloroethane
Trichloroethylene
Tetrachloroethylene
Phenol
Benzene
Toluene
Ethyl Senzer.e
Xylenes
Methylene Chloride
996
>147
.
33
30
-
<10
12
-
52
240
1,010
-
-
<5
<5
-
-
-
.
-
-
<5
1,030
-
-
-
100
<100
<100
_
-
-
-
-
-
997 996
99 >147
_
6 <5
<10 <9
-
<10 <5
8 <5
- -
20 13
229 <5
148 23
- -
-
<5 <6
15 <5
-
.
_
_ _
-
-
82 <5
37 391
-
-
-
<100 <100
<100 <100
<100 <100
- -
-
-
-
-
-
999
>U7
_
<5
81
-
<5
<5
_
6
23
81
—
-
<6
<5
-
_
-
_
_
_
<5
511
-
-
.
<100
<100
<100
.
.
-
-
-
-
1000
>147
«.
19
38
-
<5
12
_
47
137
625
-
-
<6
<5
-
.
-
_
.
-
<5
762
-
-
-
100
<100
<100
_
-
-
-
-
-
1001
>147
_
10
42
_
<5
<5
~.
106
139
273
-
_
<6
<5
_
_
_
_
..
_
<5
264
-
_
_
900
200
2,000
_
_
_
-
-
-
1002
120
_
<5
17
_
<5
<5
_
8
19
14
_
_
<6
<5
_
_
_
.
_
»
<5
30
-
.
_
8,200
<100
3.000
^
_
_
-
-
-
1003
>147
—
25
1.150
_
6
500
w
465
404
2.960
_
.
86
<5
_
v
-
—
—
.
559
268
_
_
_
1,700
<100
2.200
_
_
_
_
-
-
PSAs
Naphthalene
Penanthrene/Anthracene
Pyrene
Benzo(a)anthracene
Benzo(a)pyrene
Alkylbenzene (CgH,,)
Alkylnaphthalene tC.-H.,)
Phosphorus
Chlorine, wt Z
Sulfur, ut %
PCBs
0.12
0.07
0.01
0.08
0.07
<5
0.61
<50
0.77
<5
0.24
6
* Table A-2 identifies the sourc'e of analytical data for each used oil sample. Table A-3 provides codes
for each sample number which describes the specific generating source of used oil and the end-use.
A-122
-------
TABLE A-l (continued)
ANALYTICAL DATA FOR USED OIL SAMPLES
Sample Number*
Flash Point (CF)
Metals
Aluminum
Arsenic
Barium
Beryllium
Cadmium
Chromium
Cobalt
Copper
Iron
Lead
Magnesium
Manganese
Mrlybdenun
1004
72
<5
312
12
23
92
44
11
<5
1005
131
<5
240
7
104
56
18
<5
<5
109
19
39
161
94
<5
<5
1007
>147
<5
65
65
198
302
78
<5
<5
1008
XL47
<5
93
55
219
1,250
423
12
20
11
23
83
456
7
46
21
95
238
<5
<5
20
46
8
39
139
836
8
<5
Selenium
Silicon
Silver
Tin
Titanium
Vanadium
Zinc
<5
693
<5
1,150
<5
189
<5
78
8
221
<5
490
<5
206
<5
667
Volatile Organics
Dichlcrocifluoromethane
Trichlorofluoromethane
Trichlorocnfluoroe thane
1,1, i-Irichloroethane
Trichloroethylene
Tetrachloroethylene
Phenol
Benzene
Ztnyi Benzene
Xylenes
Methylene Chloride
PNAs
Naphthalene
Penanthrene/Anthracene
Pyrene
Benzo(a)anthracene
Ber.zo(a)pyrene
3,800 500
2.200 2,800
500 1,400
<100
<100
<100
<100
<100
<100
<100
<100
<100
<100
<100
<100
400 200
300 200
3,200 100
Alkylnapnthalene tc.-H^-)
Phosphorus
Chlorine, wt %
Sulfur, wt %
PCBs
0.42
0.32
0.40
16
0.47
38
0.19
83
0.45
64
2.25 0.16
* Table A-2 identifies the source of analytical data for each used oil sample. Table A-3 provides codes
:or each sample number which describes the specific generating source of used oil and the end-use.
A-l 23
0295
-------
TABLE A-l (continued)
ANALYTICAL DATA FOR USED OIL SAMPLES
Sample Number*
Flash Point (=F)
1012
>147
1013
>147
X014
>147
1015
>147
1016
>147
1017
>147
1018
>147
1019
>.147
Metals
Aluminum
Arsenic
Barium
Beryllium
Cadmium
Chromium
Cobalt
Copper
Iron
Lead
Magnesium
Manganese
Molybdenum
Nickel
Selenium
Silicon
Silver
Sodium
Tin
Titanium
Vanadium
Zinc
Volatile Organics
Dichlorodifluoromethane
Trichlorofluoromethane
Trichlorotrifluoroethane
1,1,1-Trichloroethane
Trichloroethylene
Tetrachloroethylene
Phenol
Benzene
Toluene
Etnyl Benzene
Xylenes
Methylene Chloride
PNAs
Naphthalene
Penanthrene/Anthracene
Pyrene
Benzo(a)anthracene
Benzo(a)pyrene
58
68
10
521
<5
14
<5
41
26
12
35
<5
8
<5
21
<5
6
27
<5
8
<5
<5
764
<5
21
<100 <100
1,500 12,000
<100 <100
<5
93
<100
<100
<100
Alkylbenzene (C.H
Alkylnaphthaler.e
Phosphorus
Chlorine, vt Z
Sulfur, wt 7.
PCBs
I2r'12'
< 5
399
50
95
2,150
3,250
14
23
27
51
44
158
856
<5
<5
24
25
<5
25
115
671
<5
<5
18
30
22
118
592
<5
<5
26
41
10
32
148
942
<5
<5
23 <5
2,030 730
1,600 <100
40,000 <100
<100 <100
<5
546
<100
<100
<100
<5
558
<5
830
<100 <100
<100 <100
<100 1.200
0.55
0.96
0.46
2.29
0.10
0.10
<5
0.21
0.14
* Table A-2 identifies the source of analytical data for each used oil sample. Table A-3 provides codes
for each sample number which describes the specific generating source of used oil and the end-use.
A-124
-------
TABLE A-l (continued;
ANALYTICAL DATA FOR USED OIL SAMPLES
Sample Number*
Flash Point CD
1020
>147
1021
>147
1022
>147
1023
>147
1024
>147
1025
>147
1026
>126
1027
>147
Metals
Aluminum
Arsenic
Barium
Beryllium
Cadmium
Chromium
Cobalt
Copper
Iron
Lead
Magnesium
Manganese
Molybdenum
Nickel
Selenium
Silicon
Silver
Sodium
Tin
Titanium
Vanadium
Zinc
Volatile Organics
Dichlorodifluoromechane
Trichlorofluoromethane
Trichlorotrifluoroethane
1,1,1-Tr ichloroe thane
Trichloroechylene
Tetrachloroethylene
Phenol
Benzene
Toluene
Etnyl Benzene
Xylenes
Methylene Chloride
PNAs
Naphthalene
Penanchrene/Anthracene
Pyrene
Benzo(a)anthracene
Benzo(a)pyrene
16
26
10
77
443
27
36
30
155
803
<5
<5
19
32
10
150
572
<5
<5
23
39
31
156
725
<5
<5
<5
428
<5
804
<100 <100
<100 <100
1,700 <100
<5
500
400
200
200
<5
622
Alkylbenzene (C,H
Alkylnaphthalene
Phosphorus
Chlorine, wt Z
Sulfur, wt %
PCBs
"12
0.13
0.10
0.27
0.36
<5
24
68
8
61
160
1,050
<5
<5
<5
788
2,200 1,100
600 1,200
<100 4.600
19
50
8
32
159
647
<5
<5
8
42
B
32
148
693
<5
<5
19
38
13
21
270
750
<5
<5
<5
694
<5
628
<5
683
400 2,600 <100
<100 1,800 <100
200 19,000 5.800
0.12
<5
2.96
<5
0.79
* Table A-2 identifies the source of analytical data for each used oil sample. Table A-3 provides codes
for each sample number which describes the specific generating source of used oil and the end-use.
A-125
029G
-------
TABLE A-i
ANALYTICAL DATA FOR USED OIL SAMPLES
Sample Number*
Flash Point (°F)
Metals
Aluminum
Arsenic
Barium
Beryllium
Cadmiun
Chromium
Cobalt
Copper
Iron
Lead
Magnesium
Manganese
Molybdenum
Nickel
Seleniur.
Silicon
Silver
Sodium
Tin
Titanium
Vanadium
Zinc
Volatile Organics
Dichlorodifluorooechane
Trichlorofluoromethane
Tnchlorotrif luoroethane
1 . 1 , 1-Trichloroethane
Tnchloroethylene
Tetrachloroethylene
Phenol
Benzene
Toluene
E:h-.-; Benzene
Xyleaes
Methylene Chloride
1028
>147
-
19
34
-
<10
<5
-
49
202
785
-
-
<5
<5
-
-
-
-
.
-
<5
864
-
-
-
8,400
<100
1,200
-
-
-
-
-
-
1029
>147
.
,28
39
-
<10
6
-
35
175
1,040
-
-
6
<5
-
-
-
-
-
-
<5
1.020
-
-
-
500
<100
200
—
-
-
-
-
-
1030
>147
-
19
28
-
<10
<5
-
11
194
555
-
-
<5
<5
-
-
-
-
_
-
<5
321
-
-
-
3,400
300
5,800
-
-
-
_
-
-
1031
>147
-
94
160
-
<10
<5
_
11
1.410
2.480
-
-
7
11
-
.
_
-
_
_
12
2,670
-
-
-
1,100
200
1,500
_
-
-
-
-
-
1032
>147
_
9
243
_
<10
66
_
40
992
786
-
-
14
17
_
-
-
-
_
_
7
1,480
-
_
.
800
500
1,100
-
-
-
_
-
-
1033
>147
_
26
38
_
<10
<5
—
37
160
1,010
-
_
6
<5
_
_
.
_
_
_
<5
848
_
_
-
700
300
300
_
_
.
_
-
-
1034
>147
_
32
32
—
<10
<5
_
36
151
932
_
_
5
<5
»
_
_
_
_
_
<5
625
_
_
_
2.600
400
2.200
_
_
_
_
-
-
1035
>147
—
17
45
. ,
<10
10
—
50
180
826
_
_
<5
<5
_
.
„
^,
—
w
<5
716
.
^
_
2,400
3,000
8,200
_
_
—
_
-
-
PNAs
Naphthalene
Penanthrene/Anthracene
Pyrene
Benzo(a)anthracene
Benzo(a)pyrene
Alkylbenzene (Cgfc
AlkyInaphthalene
Phosphorus
"12
Chlorine,
wt Z
0.29 0.10 1.06 0.09 0.22 0.20
0.25
1.85
Sulfur , ut % ________
PCBs
<5
<5
* Table A-2 identifies the source of analytical data for each used oil sample. Table A-3 provides codes
ror eacr. sample number which describes the specific generating source of used oil and the end-use.
A-126
-------
ANALYTICAL DATA FOR USED OIL SAMPLES
Sample Table*
Flash Point (T) .
Metals
Aluminum
Arsenic
Barium
Beryllium
Cadmium
Chromium
Cobalt
Copper
Iron
Lead
Magnesium
Manganese
Molybaer.'-r:
Nicicel
Selenium
Silicon
Silver
Sodium
Tin
Titanium
Vanadium
Zinc
Volatile Organics
Dichlorod if luorome thane
Trichlorofluorome thane
Tr ichlorotr if luoroe thane
1,1,1-Inchloroethane
Tnchloroethvlene
Tetracnioroethylene
Phenol
Benzene
Toluene
Ethyl Benzene
Xvlenes
Meth;. lene Chloride
1036
>147
-
22
37
-
<10
6
—
57
167
864
-
-
<5
<5
-
-
-
-
-
-
<5
709
-
-
-
4,200
200
1,100
-
-
-
-
-
-
1037
>147
-
<5
85
-
<10
25
_
27
615
177
-
-
<5
8
-
-
-
-
-
-
10
273
-
-
-
1,300
<100
32.000
-
-
-
•
-
-
1036 1039
135
-
<5 17
19 40
-
<10 <10
<5 27
-
7 24
48 146
5 558
-
-
<5 <5
<5 <5
-
-
-
-
-
-
<5 <5
15 527
-
-
-
4,200
1,900
2,000
- -
-
-
-
-
-
1040
136
_
29
50
-
<10
18
_
39
297
885
-
-
7
<5
-
-
-
-
-
-
10
728
—
-
-
5,200
1,600
2,400
-
-
-
-
-
-
1041
>147
_
24
30
-
<10
16
_
41
146
771
.
-
<5
<5
-
-
-
-
-
-
<5
575
-
-
.
6,000
900
2,800
-
-
-
~
-
-
1042
>147
_
~i "i
40
-
<10
12
_
41
143
901
-
_
<5
<5
-
-
-
-
-
_
<5
631
_
-
_
14,000
600
2,600
—
-
-
-
-
-
1043
108
_
11
40
-
<10
16
_
44
155
603
.
-
<5
<5
-
-
-
-
-
-
<5
1 525
t
_
_
_
14,000
3,000
6,800
-
-' -
-
-
_
-
PN'As
Naphthalene
Penantnrene/Anthracene
Pyrene
Benzo(a)anthracene
Benzo(a)pyrene
Alkylbenzene (CgH.,)
Alkylnaphthalene TC.,H..)
Phosphorus
Chlorine, wt %
Sulfur, wt X
PCBs
0.56
<5
2.74
0.46
0.95
1.04
1.00
1.44
l.lk
* Table A-2 identifies the source of analytical data for each used oil sample. Table A-3 provides codes
for each sample number which describes the specific generating source of used oil and the end-use.
A-127
0297
-------
TABLE A-l (continued)
ANALYTICAL DATA FOR USED OIL SAMPLES
Sample N\aiber*
Flash Point (*F)
Metals
Aluminum
Arsenic
Barium
Beryllium
Cadmium
Chromium
Cobalt
Copper
Iron
Lead
Magnesium
Manganese
Molybdenum
Nickel
Selenium
Silicon
Silver
Sodium
Tin
Titanium
Vanadium
Zinc
Volatile Organics
Dichlorodifluoromethane
trichlorof luor omethane
Trichlorotrif luoroethane
1 > 1 , 1-Tr ichloroe thane
Trichloroethylene
Tetrachloroethylene
Phenol
Benzene
Toluene
Ethyl Benzene
Xylenes
Methylene Chloride
1044
135
-
22
40
-
<10
16
—
44
159
637
-
-
<5
<5
-
-
-
-
-
-
<5
664
-
-
-
3,300
900
r.soo
-
.
-
-
-
-
1045
66
-
<5
<5
-
<10
<5
.
<5
11
17
-
-
<5
<5
-
-
-
-
-
-
<5
5
-
-
-
3,400
<100
600
-
-
-
-
-
-
j.046
64
_
<5
20
-
<10
<5
_
<5
11
21
-
-
<5
<5
-
-
-
-
-
-
<5
6
-
-
.
2,000
<100
400
-
-
-
-
-
-
1047
115
.
<5
<5
-
<10
<5
_
<5
10
24
-
-
<5
<5
-
-
-.
-
-
-
<5
65
-
-
-
1,800
700
1.200
-
-
-
-
-
-
1048
120
_
21
40
-
<10
28
»
40
170
688
-
-
<5
<5
-
-
_
-
-
-
<5
530
_
-
-
6,600
700
1,300
-
-
-
-
-
-
1049
>147
_
<5
170
_
10
35
_
126
1,250
1.820
-
-
10
7
«
-
„
_
_
_
29
1,770
_
-
-
200
<100
200
.
_
-
-
-
-
1050
>147
—
18
180
_
<10
56
—
138
367
531
.
_
<5
<5
_
_
.
_
_
_
34
591
_
-
_
2,600
200
700
.
_
.
-
-
-
1051
113
—
20
50
_
<10
18
^
35
185
656
_
_
<5
<5
_
.
_
_
_
*
15
478
_
-
_
4,600
500
700
.
_
_
-
-
-
PSAs
Naphthalene
Penanthrene/ Anthracene
Pyrene
Benzo (a) anthracene
Benzo(a)pyrene
Alkylbenzene (C.H.
Alkylnaphthalene t
)
Phosphorus
Chlorine, wt Z
Sulfur, wt 2
PCBs
--._.._
0.77 0.16 0.10 0.17 0.87 0.15
_______
<10 4 2 <1 <10 <10 <10
-
0.91
-
* Table A-2 identifies the source of analytical data for each used oil sample. Table A-3 provides codes
for each sample number which describes the specific generating source of used oil and the end-use.
A-l 28
-------
ANALYTICAL DATA FOR USED OIL SAMPLES
Sample Number*!
Flash Point (°F)
Metals
Aluminum
Arsenic
Barium
Beryllium
Cadmiuc
Chromium
Cobalt
Copper
Iron
Lead
Magnesium
Manganese
Molybdenum
Nickel
Seleniur.
Silicon
Silver
Sodium
Tin
Titaniun
Vanadiuc
Zinc
Volatile Organics
Dichlorodifluoromethane
Trichlcrof luoromethane
Trichlorocrif luoroe thane
1 ,1,1-Trichloroethane
Trichloroetnylene
Tetracnloroethylene
Phenol
Benzene
Toluene
Ethvl Benzene
Xy.er.ss
Methylene Chloride
1052
>147
-
12
20
-
<10
<5
-
<7
7
<5
-
-
10
<5
-
-
-
-
—
-
<5
8
-
-
-
<100
<100
<100
-
-
-
-
-
-
1053
>147
-
13
190
-
10
35
-
91
1,440
2.180
-
-
7
7
-
-
-
-
—
-
38
1,870
-
-
-
2,800
200
800
- •
-
-•
-
-
-
1054
>147
-
16
90
-
<10
84
-
174
126
6-: 6
-
•*
<5
<5
-
-
-
-
•*
-
<5
269
-
-
-
6,200
800
1,400
-
-
-
-
-
-
1055
135
-
22
40
-
<10
29
-
146
205
768
-
- .
<5
<5
-
-
-
-
—
-
5
514
-
-
-
3,000
600
600
-
-
-
-
-
-
1056(80) 1057(81)
>200
45
<5
67
<0.2
1.1
6.1
<0.5
33
300
890
150
10
3.3
_
„
110
—
5
310
-
-
-
1.800
460
400
-
150
2,000
430
820
250
<85
7.6
<5
25
<0.2
0.66
1.9
<0.5
25
130
440
23
3
1.4
_
_
11
_
3.7
370
-
-
-
450
120
800
-
12,000
8,000
4,000
25,000
1,400
1058(82)
>200
16
<5
35
<0.2
2.9
2.2
<0.5
26
99
560
74
4.6
1.1
9.1
1.5
730
-
-
-
1,500
390
380
-
160
670
200
500
12
1059(83
>200
23
<5
47
3.7
2. 8
<0.5
27
110
770
110
5.7
1.2
21
0.79
860
-
-
-
1,000
<4
15
-
240
810
270
50C
7
PNAs
Naphthalene
Penan threne/ Anthracene
Pyrene
Benzo (a) anthracene
Benzo(a)pyrene
AlKylbenzene (Cg
Alkylnaphthalene
Phosphorus
Chlorine, wt %
Sulfur, wt Z
PCBs
' 640
0.12 0.29 0.68 0.51 0.07
0.63
440
0.21
<°5'37
660
0.33
710
0.1
* Table A-2 identifies the source of analytical data for each used oil sample. Table A-3 provides codes
for each sample number which describes the specific generating source of used oil and the end-use.
t Numbers in parentheses represent EPA sample numbers for used oil samples obtained as part of their
1983 sampling program.
A-129
0298
-------
ANALYTICAL DATA FOR USED OIL SAMPLES
Flash Point (°F)
Metals
Aluminum
Arsenic
Barium
Beryllium
Cadmium
Chromium
Cobalt
Copper
Iron
Lead
Magnesium
Manganese
Molybdenum
N'ickel
Selenium
Silicon
Silver
Sodium
Tin
Titanium
Vanadium
Zinc
Volatile Organics
Dichlorodifluoromethane
Trichlorofluoromethane
Trichlorotrifluoroethane
1,1,1-Trichloroethane
Trichloroethylene
Tetrachloroethylene
Phenol
Benzene
Toluene
Xylenes
Methylene Chloride
PSAs
Naphthalene
Phenanthrene/Anthracene
Pyrer.e
Benzo(a)anthracene
Benzo(a)pyrene
Alkylbenzene (C
Alkylnaphthalene
Sample Number* t
1060 (84) 1061 (85) 1062 (86) 1063 (358) 1064 (361) 1065 (306)
>200 >200 >200 >200 104
3.6
<5
13
<0.2
0.93
1.6
<0.5
16
97
610
76
2.6
16
<5
52
<0.2
4.1
2.9
<0.5
27
100
720
170
5.9
11
<5
<0.5
<0.2
1.7
2.1
<0.5
7.6
75
<5
3.7
0.59
<1
<5
<0.5
<0.2
0.83
9.5
0.73
<0.5
130
<5
1.5
<0.2
2.1
48
4.2
520
<1
35
0.36
820
11
<0.2
3.7
3.2
<0.2
2.4
3,500
<4
4
97
640
200
7
<4 .
44
<2
3
3
86
88
111
<2
140
<1
-------
ANALYTICAL DATA FOR USED OIL SAMPLES
Sample Number* t
Flash Point (*F)
Metals
Aluminum
Arsenic
Barium
Beryllium
Cadmium
Chromium
Cobalt
Copper
Iron
Lead
Magnesium
Manganese
Mciyocenua
Nickel
Selenium
Silicon
Silver
Sodium
Tin
Titanium
Vanadium
Zinc
Volatile Organics
Dichlorodif luoromethane
Trichlorof luoromethane
Trichlorotrifluoroe thane
1,1, 1-Trichloroe thane
Trichloroethylene
Tetrachloroethylene
Phenol
Benzene
Toluene
Ethyl Benzene
Xyler.cs
Methylene Chloride
1066 (34)
-
980
<5
3.2
<0.2
<0.5
1.5
<0.5
<0.5
5.1
<5
0.69
0.34
-
<1
-
-
-
2.1
-
-
0.2
2.6
-
-
-
<20
<20 26
<20
-
<20
230
<20
<20
<20 26
1067 (36) 1068 (37) 1069 (50) 1070:54)
-
<1
<5
3.2
<0.2
<0.5
6.7
3.5
18
74
100
0.99
49
-
8.1
-
-
-
11
-
-
<0.2
38
-
.
-
<20
,000
<20
-
<20
<20
670
560
,000
-
8.7
<5
120
<0.2
<0.5
2.8
<0.5
3.4
87
<5
15
3.5
-
<1
-
-
-
2.4
-
_
0.49
10
-
-
-
<8
<8
<8
-
<8
<8
<8
<8
<8
>200
53
<5
8.5
<0.2
<0.5
7
<0.5
5.4
350
13
17
2
-
<1
_
-
.
1,800
-
_
<0.2
3.9
-
_
-
<7.4
<7.4
<7.4
-
<7.4
<7.4
<7.4
<7.4
<7.4
-
<1
<5
1.1
<0.2
<0.5
<0.5
<0.5
14
8.2
16
<0.5
0.49
-
1.5
_
_
-
1.3
-
_
<0.2
23
-
_
-
<16
<16
<16
-
<16
<16
<16
<16
<16
1071(59)
>200
16
<5
8.5
<0.2
<0.5 -"
0.82
0.93
19
110
6.9
0.56
0.62
-
1.1
_
_
-
2.4
-
_
<0.2
14
-
_
_
<32
<32
<32
-
<32
57
<32
<32
<32
PNAs
Naphthalene
Penanthrene/Anthracene
Pyrene
Benzo(a)anthracene
Benzo(a)pyrene
Alkylbenzene (CqH..,)
Alkylnaphthalene tc,,H,,)
Phosphorus
Chlorine, wt 2
Sulfur, wt Z
PCBs
300
<0.01
<5
580
0.93
<5
280
2
<5
380
0.02
0.51
<5
110
0.01
<5
270
0.65
<5
* Table A-2 identifies the source of analytical data for each used oil sample. Table A-3 provides codes
for each sample number which describes the specific generating source of used oil and the end-use.
+ Numbers in parentheses represent EPA sample numbers for used oil samples obtained as part of their
1983 sampling program.
A-132
0293
-------
TABLE A-2
SOURCE KEY FOR USED OIL SAMPLES IN TABLE A-l
Sample
Number
1-7
8
9
10
11-20
21
22-43
except 26
26
44
45
46
47
48
49
50
51
52-63
Source
A-l
A-12
A-12
A-10
A-2
A-13
A-15
A-21
A-17
A-26
A-27
A-28
A-29
A-30
A- 34
A-32
A-38
Date of
Publication
or Analysis
1982
1976
1981
Unknown
1977
1972
1977
1982
1979
1977
1977
1974
1974
1976
1981
1980
1978
A-133
-------
TABLE A-2 (continued)
SOURCE KEY FOR USED OIL SAMPLES IN TABLE A-l
Sample
Number
64
65-66
67-69
70-72
73-92
93-94
95-112
113-134
135-137
138
139
140
141
142
143
144
145
146
147
Source
A-39
A-36
A-37
A-48
A-32
A-24
A-24
A-24
A-19
A-l 9
A-19
A-19
A-19
A-19
A-19
A-19
A-19
A-19
A-40
Date of
Publication
or Analysis
1982
1982
1974
1983
1980
1978
1978
1978
Unknown
Unknown
1978
1978
1978
1978
1978
1978
1978
1978
1982
A-134
0300
-------
TABLE A-2 (continued)
SOURCE KEY FOR USED OIL SAMPLES IN TABLE A-l
Sample
Number
148
149
150
151
152
153
154
155
156
157
158
159
160
161-162
163-176
177
178
179
180-236
Source
A-40
A-40
A-40
A-40
A-40
A-40
A-40
A-40
A-40
A-40
A-40
A-40
A-40
A-25
A-49
A-5
A-10
A-10
A-20
Date of
Publication
or Analysis
1982
1982
1982
1982
1982
1982
1982
1982
1982
1982
1982
1982
1982
1977
1983
1982
Unknown
Unknown
1979-1981
A-135
-------
TABLE A-2 (continued)
SOURCE KEY FOR USED OIL SAMPLES IN TABLE A-l
Sample
Number
237-243
244
245
246-253
254-258
259-260
261
262-263
264-266
267
268
269-315
316-317
318-334
335-404
405-431
432-459
460-481
Source
A-l
A-3
A-4
A-9
A-20
A-7
A-ll
A-9
A-5
A-22
A-22
A-23
A-35
A-8
A-20
A-42
A-4 3
A-44
Date of
Publication
or Analysis
1982
1977
1979
1981
1981
1981
1979
1981
1982
1982
1982
1982
1982
1982
1979 to 1981
1982
1982
1982
A-136
0301
-------
TABLE A-2 (continued)
SOURCE KEY FOR USED OIL SAMPLES IN TABLE A-l
Sample
Number
482-490
491-568
569-578
579-589
590
591
592-659
660-669
670-737
738-771
772-839
840-879
880-1055
Source
A-45
A-49
A-32
A-9
A-47
A-47
A-48
A-46
A-48
A-49
A-48
A-50
A-49
Date of
Publication
or Analysis
1982
1983
1980
1981
1982
1974
1983
1983
1983
1983
1983
1978
1983
A-137
-------
TABLE A-3
USED OIL SAMPLE IDENTIFICATION CODES
SAMPLE
NUMBER
1
2
3
4
5
6
7
8
9
10
11
12
13
14
15
16
17
18
19
20
21
22
23
24
25
26
27
28
29
30
31
32
33
34
35
36
37
38
39
40
CODE*
C, J
C, J
C, J
C, J
C, J
C, J
C, J
B, J
B, J
B, J
B, H
B, H
B, H
B, H
B, H
B, H
B, H
B, H
B, H
C, J
C, J
B, J
B, J
B, J
B, J
C, G
B, J
B, J
B, J
B, J
B, J
B, J
B, J
B, J
B, J
B, J
B, J
B, J
B, J
B, J
SAMPLE
NUMBER
41
42
43
44
45
46
47
48
49
50
51
52
53
54
55
56
57
58
59
60
61
62
63
64
65
66
67
68
69
70 (262) t
71 (263)
72 (264)
73
74
75
76
77
78
79
80
CODE
B, J
B, J
B, J
B, J
B, J
C, H
B, J
B, J
B, J
C, G
B, J
B, H
B, H
B, H
B, H
B, H
B, H
B, H
B, H
B, H
B, H
B, H
B, H
C, G
C, J
C, J
C, J
C, J
C, J
A, C, J, K
A, C, J, K
A, C, J, K
B, G
B, G
B, G
B, G
B, G
B, G
B, G
B, G
* Letter codes are defined at end of table.
f Numbers in parentheses represent EPA sample numbers for used oil
samples obtained as part of their 1983 sampling program.
A-138
0302
-------
TABLE A-3 (continued)
USED OIL SAMPLE IDENTIFICATION CODES
SAMPLE
NUMBER
81
82
83
84
85
86
87
88
89
90
91
92
93
94
95
96
97'
98
99
100
101
102
103
104
105
106
107
108
109
110
111
112
113
114
115
116
117
118
119
120
CODE*
B, G
B, G
B, G
B, G
B, G
B, G
B, G
B, G
B, G
B, G
B, G
B, G
Dl, J
Dl, J
E4, il
E4, H
E4, H
E4, H
E4, H
E4, H
E4, H
E4, H
E4, H
E4, H
E4, H
E4, H
E4, H
E4, H
E4, H
E4, H
E4, H
E4, H
Dl, J
D4, J
Dl, J
Dl, J
D4, J
Dl, J
Dl, J
Dl, J
SAMPLE
NUMBER
121
122
123
124
125
126
127
128
129
130
131
132
133
134
135
136
137
138
139
140
141
142
143
144
145
146
147
148
149
150
151
152
153
154
155
156
157
158
159
160
CODE
Dl, J
Dl, J
Dl, J
Dl, J
Dl, J
Dl, J
Dl, J
Dl, J
Dl, J
Dl, J
Dl, J
D4, J
D4, J
DA, J
D4, J
D4, J
D4, J
Dl, J
Dl, J
D4, J
D4, J
D4, J
D4, J
D4, J
D4, J
D3, J
Dl, J
Dl, J
D3, J
Dl, J
Dl, J
Dl, J
D2, J
Dl, J
Dl, J
Dl, J
D4, J
Dl, J
Dl, J
Dl, J
* Letter codes are defined at end of table.
A-139
-------
TABLE A-3 (continued)
USED OIL SAMPLE IDENTIFICATION CODES
SAMPLE
NUMBER
161
162
163
164
165
166
167
168
169
170
171
172
173
174
175
176
177
178
179
180
181
182
183
184
185
186
187
188
189
190
191
192
193
194
195
196
197
198
199
200
CODE*
D4, J
D4, J
E4, G
E4, G
E4, G
E4, G
E4, G
E4, G
E4, G
E4, G
E4, G
E4, G
E4, G
E4, G
E4, G
E4, G
D4, J
D4, J
D4, J
F, I
F, I
F, I
F, I
F, I
F, I
F, I
F, I
F, I
F, I
F, I
F, I
F, I
F, I
F, I
F, I
F, I
F, I
F, I
F, I
F, I
SAMPLE
NUMBER
201
202
203
204
205
206
207
208
209
210
211
212
213
214
215
216
217
218
219
220
221
222
223
224
225
226
227
228
229
230
231
232
233
234
235
236
237
238
239
240
CODE
F, I
F, I
F, I
F, I
F, I
F, I
F, I
F, I
F, I
F, I
F, I
F, I
F, I
F, I
F, I
F, I
F, I
F, I
F, I
F, I
F, I
F, I
F, I
F, I
F, I
F, I
F, I
F, I
F, I
F, I
F, I
F, I
F, I
F, I
F, I
F, I
F, J
F, J
F, J
F, J
Letter codes are defined at end of table.
A-140
0303
-------
TABLE A-3 (contintied)
USED OH. SAMPLE IDENTIFICATION
SAMPLE
»uriBER
241
242
243
244
245
246
247
248
249
250
251
252
253
254
255
256
257
258
259
260
261
262
263
264
265
266
267
268
269
270
271
272
273
274
275
276
277
278
279
280
CODE*
F, J
F, J
-F. J
F, J
F, J
F, T>
F, D
F, D
F, D
F, D
T. D
F, JD
F, D
F, D
F, D
F, D
F, D
F, D
F, I
F, I
F, I
F, T
F, I
F, H
F, B
F, H
F, H
F, H
F, H
F. H
F. H
F. H
F, H
F, H
F, H
F, H
F, H
F, H
T, B
T, H
SAMPLE
UUMBER
281
282
283
284
285
286
287
288
289
290
291
292
293
294
295
296
297
298
299
300
301
302
303
304
305
306
307
308
309
310
311
312
313
314
315
316
317
318
319
320
CODES
CODE
F, G
F, G
F, G
F, G
F, G
F, G
F, G
F, G
F, G
F, G
F, G
F, G
F, G
F, G
F, G
F, G
F, G
F, G
F, G
F, G
F, G
F, G
F, G
F, G
F, G
F, G
F, G
F, G
F, G
F, G
F, G
F, G
F, G
F, G
F, G
F, G
F, G
F, P
F, P
F, P
Letter codes are defined at end of table.
A-141
-------
TABLE A-3 (continued)
USED OIL SAMPLE IDENTIFICATION CODES
SAMPLE
NUMBER
321
322
323
324
325
326
327
328
329
330
331
332
333
334
335
336
337
338
339
340
341
342
343
344
345
346
347
348
349
350
351
352
353
354
355
356
357
358
359
360
CODE*
F, P
F, P
F, P
F, P
F, P
F, P
F, P
F, P
F, P
F, P
F, P
F, P
F, P
F, D
F, I
F, I
F, I
F, I
F, I
F, I
F, I
F, I
F, I
F, I
F, I
F, I
F, I
F, I
F, I
F, I
F, I
F, I
F, I
F, I
F, I
F, I
F, I
F, I
F, I
F, I
SAMPLE
NUMBER
361
362
363
364
365
366
367
368
369
370
371
372
373
374
375
376
377
378
379
380
381
382
383
384
385
386
387
388
389
390
391
392
393
394
395
396
397
398
399
400
CODE
F, I
F, I
F, I
F, I
F, I
F, I
F, I
F, I
F, I
F, I
F, I
F, I
F, I
F, I
F, I
F, I
F, I
F, I
F, I
F, I
F, I
F, I
F, I
F, I
F, I
F, I
F, I
F, I
F, I
F, I
F, I
F, I
F, I
F, I
F, I
F, I
F, I
F, I
F, I
F, I
* Letter codes are defined at end of table.
A-142
0304
-------
TABLE A-3 (continued)
USED OIL SAMPLE IDENTIFICATION CODES
SAMPLE
NUMBER
401
402
403
404
405
406
407
408
409
410
411
412
413
414
415
416
417
418
419
420
421
422
423
424
425
426
427
428
429
430
431
432
433
434
435
436
437
438
439
440
CODE*
F, I
F, I
F, I
F, I
F, G
F, G
F, G
F, G
F, G
F, G
F, G
F, G
F, G
F, G
F, G
F, G
F, G
F, G
F, G
F, G
F, G
F, G
F, G
F, G
F, G
F, G
F, G
F, G
F, G
F, G
F, G
F, G
F, G
F, G
F, G
F, G
F, G
F, G
F, G
F, G
SAMPLE
NUMBER
441
442
443
444
445
446
447
448
449
450
451
452
453
454
455
456
457
458
459
460
461
462
463
464
465
466
467
468
469
470
471
472
473
474
475
476
477
478
479
480
CODE
F, G
F, G
F, G
F, G
F, G
F, G
F, G
F, G
F, G
F, G
F, G
F, G
F, G
F, G
F, G
F, P
F, P
F, G
F, G
F, G
F, G
F, G
F, G
F, G
F, G
F, G
F, G
F, G
F, G
F, G
F, G
F, G
F, G
F, G
F, G
F, G
F, G
F, G
F, G
F, G
* Letter codes are defined at end of table.
A-143
-------
TABLE A-3 (continued)
USED OIL SAMPLE IDENTIFICATION CODES
SAMPLE
NUMBER
481
482
483
484
485
486
487
488
489
490
491
492
493
494
495
496
497
498
499
500
501
502
503
504
505
506
507
508
509
510
511
512
513
514
515
516
517
518
519
520
CODE*
F,
F,
F,
F,
F,
F,
F,
F,
F,
F,
F,
F,
F,
F,
F,
F,
F,
F,
F,
F,
F,
F,
F,
F,
F,
F,
F,
F,
F,
F,
F,
F,
F,
F,
F,
F,
F,
F,
F,
F,
G
G
G
G
G
G
G
G
G
G
G,
G,
G,
G,
G,
G,
G,
G,
G,
G,
G,
G,
G,
G,
G,
G,
G,
G,
G,
G,
G,
G,
G
G
G,
G
G
G
G
G,
L
L
L
L
L
L
L
L
R
K
R
L
L
L
L
L
L
L
L
R
R
L
R
L
SAMPLE
NUMBER
521
522
523
524
525
526
527
528
529
530
531
532
533
534
535
536
537
538
539
540
541
542
543
544
545
546
547
548
549
550
551
552
553
554
555
556
557
558
559
560
CODE
F
F
F
F
F
F
F
F
F
F
F
F
F
F
F
F
F
F
F
F
F
F
F
F
F
F
F
F
F
F
F
F
F
F
F
F
F
F
F
F
9
9
9
9
9
9
9
9
9
9
9
9
9
9
9
9
9
9
9
9
9
9
9
9
9
9
9
9
9
9
9
9
9
9
9
9
9
9
9
9
G
G
G
G
G
G
G
G
G
G
G
G
G
G
G
G
G
G
G
G
G
G
G
G
G
G
G
G
G
G
G
G
G
G
G
G
G
G
G
G
9
9
9
9
9
9
f
9
9
9
9
9
9
9
9
9
9
9
»
9
9
9
9
9
9
9
9
9
9
9
9
9
9
9
9
9
9
9
9
9
L
L
L
L
L
L
R
R
R
L
L
L
L
L
R
R
R
R
R
R
R
R
R
R
L
L
L
L
L
R
R
R
R
R
R
R
R
K
R
R
* Letter codes are defined at end of table.
A-144
0305
-------
TABLE A-3 (continued)
USED OIL SAMPLE IDENTIFICATION CODES
SAMPLE
NUMBER
561
562
563
564
565
566
567
568
569
570
571
572
573
574
575
576
577
578
579
580
581
582
583
584
585
586
587
588
589
590
591
592 (H0)t
593 (111)
594 (112)
595 (118)
596 (119)
597 (120)
598 (121)
599 (123)
600 (124)
CODE*
F,
F,
F,
F,
F,
F,
F,
F,
F,
F,
F,
F,
F,
F,
F,
F,
F,
F,
F,
F,
F,
F,
F,
F,
F,
F,
F,
F,
F,
F,
F,
A,
A,
A,
A,
A,
A,
A,
A,
A,
G,
G,
G,
G,
G,
G,
G,
G,
H
H
H
H
H
H
H
H
H
H
J
J
J
J
J
J
J
J
J
J
J
I
J
B,
B,
B,
B,
D3
B,
B,
B,
B,
K
K
K
K
K
K
K
K
J, K
J, K.
J, K
J, K
, K, J
J, K
J, K
J > K
J, K
SAMPLE
NUMBER
601
602
603
604
605
606
607
608
609
610
611
612
613
614
615
616
617
618
619
620
621
622
623
624
625
626
627
628
629
630
631
632
633
634
635
636
637
638
639
640
(125)
(126)
(127)
(128)
(129)
(130)
(131)
(132)
(133)
(135)
(137)
(138)
(140)
(142)
(146)
(147)
(148)
(151)
(152)
(161) .
(163)
(164)
(165)
(166)
(167)
(168)
(169)
(170)
(174)
(177)
(181)
(182)
(187)
(188)
(190)
(191)
(193)
(202)
(204)
(205)
CODE
A,
A,
A,
A,
A,
A,
A,
A,
A,
A,
A,
A,
A,
A,
A,
A,
A,
A,
A,
A,
A,
A,
A,
A,
A,
A,
A,
A,
A,
A,
A,
A,
A,
A,
A,
A,
A,
A,
A,
A,
B
B
B
B
B
B
B
B
B
F
F
F
F
F
F
F
C
C
C
F
F
F
F
F
F
F
F
F
F
F
F
F
F
F
F
F
F
F
>
t
»
>
>
»
»
»
»
>
t
>
>
»
»
»
»
t
t
*
»
>
>
t
»
t
>
t
t
»
t
f
>
»
»
t
t
>
DA
D4
J
J
J
J
J
J
J
J
J
H
H
H
H
H
H
H
G
G
G
J
J
J
J
J
I
I
I
I
I
J
J
J
J
J
J
G
J
J
»
»
»
t
•
»
»
»
t
>
»
>
>
>
>
>
>
»
»
>
>
»
»
»
t
>
f
>
>
>
«
»
>
»
>
J
J
K
K
K
K
K
K
K
K
K
K
K
L
K
K
K
K
K
K
K
K
K
K
K
K
K
K
K
K
K
K
K
K
K
, K
, K
* Letter codes are defined at end of table.
t Numbers in parentheses represent EPA sample numbers for used oil
samples obtained as part of their 1983 sampling program.
A-145
-------
TABLE A-3 (continued)
USED OIL SAMPLE IDENTIFICATION CODES
SAMPLE
NUMBER
641 (207)t
642 (208)
643 (209)
644 (233)
645 (242)
646 (243)
647 (245)
648 (250)
649 (255)
650 (256)
651 (257)
652 (258)
653 (259)
654 (261)
655 (265)
656 (267)
657 (268)
658 (271)
659 (272)
660
661
662
663
664
665
666
667
668
669
670 (13)
671 (14)
672 (15)
673 (16)
674 (60)
675 (104)
676 (105)
677 (106)
678 (107)
679 (108)
680 (109)
CODE*
A, F, J, L
A, F, J, L
A, F, J, L
A, F, J, K
A, D3, J, K
A, D4, J, K
A, D4, J, K
A, E3, J, K
A, F, J, K
A, F, J, K
A, F, J, K
A, F, J, K
A, B, J, K
A, B, J, K
A, E4, J, K
A, E4, G, K
A, F, J
A, C, H, K
A, C, J, K
F, G
F, G
F, G
F, G
F, G
F, G
F, G
F, G
F, G
F, G
A, D4, J
A, D4, J
A, D4, J
A, D4, J
A, B, G
A, F, G
A, F, G
A, F, G
A, F, G
A, F, G
A, F, G
SAMPLE
NUMBER
681 (211)
682 (212)
683 (213)
684 (218)
685 (220)
686 (227)
687 (228)
688 (230)
689 (280)
690 (281)
691 (282)
692 (284)
693 (285)
694 (288)
695 (292)
696 (294)
697 (295)
698 (296)
699 (298)
700 (299)
701 (300)
702 (301)
703 (302)
704 (303)
705 (316)
706 (319)
707 (145)
708 (171)
709 (172)
710 (173)
711 (175)
712 (176)
713 (178)
714 (179)
715 (183)
716 (184)
717 (185)
718 (186)
719 (192)
720 (194)
i
CODE
A, J, J
A, J, J
A, F, J
A, D3, J
A, D3, J
A, Dl, J
A, Dl, J
A, F, J. K
A, C, G
A, C, G
A, F, G
A, F, G
A, F, G
A, F, G
A, J, J
A, F, J
A, F, J
A, F, J
A, F, G
A, F, G
A, F, G
A, F, G
A, F, G
A, F, G
A, C, G
A, C, G
A, F, H, L
A, F, J, K
A, F, J
A, F, J, K
A, F, J
A, F, J
A, F, J, K
A, F, J, K
A, F, J, K
A, F, J
A, F, J
A, F, G, K
A, F, J, K
A, F, J, K
* Letter codes are defined at end of table.
t Numbers in parentheses represent EPA sample numbers for used oil
samples obtained as part of their 1983 sampling program.
0306
A-146
-------
TABLE A-3 (continued)
USED OIL SAMPLE IDENTIFICATION CODES
SAMPLE
NUMBER
721
722
723
724
725
726
727
728
729
730
731
732
733
734
735
736
737
738
739
740
741
742
743
744
745
746
747
748
749
750
751
752
753
754
755
756
757
758
759
760
(195)t
(197)
(198)
(200)
(201)
(203)
(206)
(223)
(224)
(225)
(232)
(244)
(251)
(252)
(253)
(254)
(270)
CODE*
A,
A,
A,
A,
A,
A,
A,
A,
A,
A,
A,
A,
A,
A,
A,
A,
A,
F,
F,
F,
F,
F,
F,
F,
F,
F,
F,
F,
F,
F,
F,
F,
F,
F,
F,
F,
F,
F,
F,
F,
F,
F,
F,
F,
F,
F,
F,
F,
C,
F,
F,
E4
C,
Dl
Dl
F,
E3
J,
J,
J,
J,
J,
J,
J,
J,
J,
J,
J,
J,
J,
J,
J,
J,
J,
J,
J,
J,
J,
J,
J,
J, R
J, R
I, K
J, R
J
J, R
J, R
H, R
H, R
H, R
G, L
, J, R
J, R
, J, R
, J, R
J, R
, J, R
R
R
R
K
R
R -
L
L
R
K
R
R
L
L
L
L
R
K
R
K
K
L
L
SAMPLE
NUMBER
761
762
763
764
765
766
767
768
769
770
771
772
773
774
775
776
777
778
779
780
781
782
783
784
785
786
787
788
789
790
791
792
793
794
795
796
797
798
799
800
(333)
(348)
(354)
(356)
(1)
(2)
(3)
(4)
(5)
(6)
(10)
(51)
(52)
(62)
(63)
(64)
(65)
(66)
(67)
(92)
(93)
(94)
(122)
(297)
(320)
(326)
(327)
(328)
(329)
CODE
F,
F,
F.
F,
F,
F,
F,
F,
F,
F,
F,
A,
A,
A,
A,
A,
A,
A,
A,
A,
A,
A,
A,
A,
A,
A,
A,
A,
A,
A,
A,
A,
A,
A,
A,
A,
A,
A,
A,
A,
J,
J,
J,
J,
J,
J,
J,
J,
J,
J,
J,
F,
B,
F,
B,
F,
F,
F,
F,
F,
F,
D4
DA
D3
F,
F,
F,
F,
F,
F,
E3
F,
C,
C,
F,
F,
C,
C,
F,
C,
L
L
R
R
R
R
R
R
R
R
R
J
H,
J,
J,
J
J
J
J
J
J
, J
» J
» J
G
G
G
G
G
G
, J
G
J,
J,
J
G
G
G
G
G
R
R
R
, R
, R
R
R
* Letter codes are defined at end of table.
t Numbers in parentheses represent EPA sample numbers for used oil
samples obtained as part of their 1983 sampling program.
A-147
-------
TABLE A-3 (continued)
USED OIL SAMPLE IDENTIFICATION CODES
-_—====
SAMPLE
NUMBER
801 (335)t
802 (337)
803 (338)
804 (339)
805 (340)
806 (341)
807 (342)
808 (343)
809 (344)
810 (345)
811 (359)
812 (360)
813 (89)
814 (90)
815 (91)
816 (95)
817 (96)
818 (98)
819 (99)
820 (101)
821 (102)
822 (103)
823 (214)
824 (216)
825 (217)
826 (226)
827 (227)
828 (234)
829 (235)
.830 (236)
831 (237)
832 (238)
833 (240)
834 (275)
835 (276)
836 (278)
837 (279)
838 (331)
839 (332)
840
CODE*
A, F, G
A, F, G
A, F, G
A, F, G
A, C, G
A, C, G
A, C, G
A, C, G
A, C, G
A, C, G
A, F, J
A, F, J
A, F, G
A, F, G
A, F, J
A, F, J, K
A, F, J, L
A, F, G, K
A, F, J, K
A, F, J, K
A, F, G, K
A, F, J, L
A, F, J, L
A, F, J, L-
A, F, J, K
A, El, J
A, Dl, J, K
A, F, G, K
A, Dl, J, K
A, Dl, J, K
A, F, G, K
A, Dl, J
A, Dl, J, K
A, D2, J
A, D2, J, K
A, D2, J
A, F, J
A, F, J
A, F, J
B, J
SAMPLE
NUMBER
841
842
843
844
845
846
847
848
849
850
851
852
853
854
855
856
857
858
859
860
861
862
863
864
865
866
867
868
869
870
871
872
873
874
875
876
877
878
879
880
CODE
B, J
B, J
B, J
B, J
B, J
B, J
B, J
B, J
B, J
B, J
B, J
B, J
B, J
B, J
B, J
B, J
B, J
B, J
B, J
B, J
B, J
B, J
B, J
B, J
B, J
B, J
B, J
B, J
B, J
B, J
B, J
B, J
B, J
B, J
B, J
B, J
B, J
B, J
B, J
C. J, K
* Letter codes are defined at end of table.
f Numbers in parentheses represent EPA sample numbers for used oil
samples obtained as part of their 1983 sampling program. 0307
A-148
-------
TABLE A-3 (continued)
USED OIL SAMPLE IDENTIFICATION CODES
SAMPLE
NUMBER
881
882
883
884
885
886
887
888
889
890
891
892
893
894
895
896 .
897
898
899
900
901
902
903
904
905
906
907
908
909
910
911
912
913
914
915
916
917
918
919
920
CODE*
C, J, R
C, J, R
C, J, K
C, J, K
C, J, L
C, J, L
C, J, K
C, J, R
C, J, R
C, J, K
C, J, K
C, J, K
C, J, K
C, J, K
C, J, K
C, H, K
C, H, K
E4, G, L
E4, G, L
E4, G, L
E4, G, L
E4, G, L *
E4, G, L
E4, G, L
E4, G, L
E4, G, L
E4, G, L
E4, G, L
E4, G, L
E4, G, K
E4, G, K
E4, G, K
E4, G, K
E4, G, R
E4, G, K
E4, G, K
E4, G, K
E4, G, K
E4, G, K
E4, G, K
SAMPLE
NUMBER
921
922
923
924
925
926
927
928
929
930
931
932
933
934
935
936
937
938
939
940
941
942
943
944
945
946
947
948
949
950
951
952
953
954
955
956
957
958
959
960
CODE
E4, G, L
E4, G, L
E4, G, L
E4, G, L
E4, G, R
E4, G, R
E4, G, R
E4, G, R
E4, G, R
E4, G, R
E4, G, R
E4, G, R
E4, G, K
£4, G, R
E4, G, R
£4, G, R
E4, H, L
E4, H, L
E4, H, R
E4, H, R
E4, H, R
E4, H, R
E4, H, R
E4, H, R
E4, H, R
E4, H, R
E4, H, R
F, I, R
F, I, R
F, I, R
F, I, R
F, I, R
F, I, R
F, I, R
F, I, R
F, I, R
F, I, R
F, I, R
F, I, R
F, I, R
* Letter codes are defined at end of table.
A-149
-------
TABLE A-3 (continued)
USED OIL SAMPLE IDENTIFICATION CODES
SAMPLE
NUMBER
961
962
963
964
965
966
967
968
969
970
971
972
973
974
975
976
977
978
979
980
981
982
983
984
985
986
987
988
989
990
991
992
993
994
995
996
997
998
999
1000
CODE*
F, I, K
F, I, K
F, I, K
F, H, K
F, H, K
F, H, K
F, H, K
F, H, K
F, H, K
F, H, K
F, H, K
F, H, K
F, H, K
F, Q, K
F, Q, K
F, Q, K
F, Q, K
F, Q, K
F, Q, K
F, Q, K
F, Q, K
F, Q, K
F, Q, K
F, Q, K
F, Q, K .
F, Q, K
F, Q, K
F, Q, K
F, Q, K
F, Q, K
F, Q, K
F, Q, K
F, Q, K
F, Q, K
F, Q, K
F, Q, K
F, Q, K
F, J, L
F, J, L
F, J, K
SAMPLE
NUMBER
1001
1002
1003
1004
1005
1006
1007
1008
1009
1010
1011
1012
1013
1014
1015
1016
1017
1018
1019
1020
1021
1022
1023
1024
1025
1026
1027
1028
1029
1030
1031
1032
1033
1034
1035
1036
1037
1038
1039
1040
CODE
F, J, K
F, J, K
F, J, K
F, J, L
F, J, L
F, J, K
F, J, K
F, J, K
F, J, K
F, J, K
F, P, L
F, P, L
F, P, L
F, P, L
F, P, L
F, P, L
F, P, L
F, P, L
F, P, L
F, P, L
F, P, L
F, P, L
F, P, L
F, P, L
F, P
F, P, K
F, P, K
F, P, K
F, P, K
F, P, K
F, P, K
F, P, K
F, P, K
F, P, K
F, P, K
F, P, K
F, P, K
F, P, K
F, J, L
F, J, L
* Letter codes are defined at end of table.
0308
-------
TABLE A-3 (continued)
USED OIL SAMPLE IDENTIFICATION CODES
SAMPLE
NUMBER
1041
1042
1043
1044
1045
1046
1047
1048
1049
1050
1051
1052
1053
1054
1055
1056 (80) t
1057 (81)
1058 (82)
1059 (83}
1060 (84)
1061 (85)
1062 (86)
1063 (358)
1064 (361)
1065 (306)
1066 (34)
1067 (36)
1068 (37)
1069 (50)
1070 (54)
1071 (59)
SAMPLE
CODE* NUMBER CODE
F, J, L
F, J, L
F, J, L
F, J, L
F, J, L
F, J, L
F, J, L
F, J, L
F, J, L
F, J, L
F, J, L
F, J, L
F, J, K
F, J, K
F, J, K
A, F, G
A, F, G
A, F, G
A, F, G
A, F, G
A, F, G
A, C, J
A, J, J
A, F, J -
A, F, J
A, El, J
A, El, J
A, El, J
A, E4, J
A, E4, J
A, E4, J
* Letter codes are defined at end of table.
t Numbers in. parentheses represent EPA sample numbers for used oil
samples obtained as part of their 1983 sampling program.
A-151
-------
TABLE A-3 (continued)
USED OIL SAMPLE IDENTIFICATION CODES
SAMPLE CODE KEY
A - Sample analyzed as part of EPA's 1983 used oil sample program
8 - Automotive oil; sample taken from generator
C - Automotive oil; sample taken from collector or processor
D - Industrial oil; sample taken from generator
Dl - Cutting or machine oils
D2 - Cooling oils
D3 - Hydraulic oils
D4 - Unknown oil types
E - Industrial oil; sample taken from collector or processor
El - Cutting or machine oils
E2 - Cooling oils
E3 - Hydraulic oils
E4 - Unknown oil types
F - Unknown oil source
G - Burned as fuel
H - Re-refined
I - Road oil
J - Unknown end-use
P - Road oil or burned as fuel
Q - Road oil or re-refined
A-152
0300
-------
-------
APPENDIX A
REFERENCES
A-l Unpublished analytical data obtained from the office of
Norman F. Surprenant, GCA Corporation, Inc., Bedford,
Massachusetts, July 1982.
A-2 U.S. Environmental Protection Agency. Assessment of indus-
trial hazardous waste management, petroleum re-refining
industry. 1977.
A-3 Reindl, J. Waste oil recycling. Journal of Environmental
Health, Vol. 40, No. 1, July/August 1977, pp. 52-55.
A-4 Linnard, R. £., and L. M. Henton. Re-refined waste oil with
PROP. Hydrocarbon Processing, September 1979, pp. 148-153.
A-5 Unpublished analytical data obtained from Thomas Manning,
Resource Technology, Inc., June 1982.
A-6 Bartlesville Energy Research Center. Waste lubricating oil
research: A comprehensive characterization of five typical
re-refinery feedstocks, Part 5. April 1977.
A-7 Stephens, R. D., et al. A study of the fate of selected
toxic materials in waste oils used for dust palliation on
logging roads in the Plumas National Forest. California
Department of Health Services. March 1981.
A-8 Unpublished analytical data obtained from Henry Aho, Maine
Department of Environmental Protection, July 6, 1982.
A-9 Nims, J., et al. An analysis of waste oil in Maine. Maine
Department of Environmental Protection. 1981.
A-10 Smith, I. C., T. L. Ferguson, and B. L. Carson. Metals in
new and used petroleum products and by-products. Midwest
Research Institute. Not dated.
A-ll Hess, L. Y. Reprocessing and disposal of waste petroleum
oils. NOYES Data Corporation, Park Ridge, New Jersey.
1979.
0310
A-153
-------
A-12 Raymond, R. L., J. O. Hudson, and V. W. Jamison. Oil degra-
dation in soil. Applied and Environmental Microbiology,
April 1976, pp. 522-535.
A-13 Freestone, F. J. Runoff of oils from rural roads treated to
suppress dust. U.S. Environmental Protection Agency.
Publication EPA-R2-72-054, October 1972.
A-14 Winters, K., and P. L. Parker. Water soluble components of
crude oils, fuel oils, and used crank-case oils. Proceed-
ings; 1977 Oil Spill Conference (Prevention, Behavior, Con-
trol, Cleanup), March 8-10, 1977, New Orleans, pp. 579-581.
A-15 Cotton, F. 0., et al. Analysis of 30 used motor oils.
Hydrocarbon Processing, September 1977, pp. 131-140.
A-16 Geyer, C., and E. Glendening. The used oil recycling program
Oregon Department of Environmental Quality. Not dated.
A-17 May, W. E., and J. M. Brown. The analysis of some residual
fuel and waste lubricating oils by a high-performance liquid
chronatographic procedure. Proceedings? Workshop on Measure-
ments and Standards for Recycled Oil, NBS, Gaithersburg,
Maryland, November 29-30, 1977. Issued September 1979.
A-18 Coyle, T. D., and A. R. Siedle. Metals in oil: Occurrence
and significance for reuse of spent automotive lubricating
oils. Proceedings? Workshop on Measurements and Standards
for Recycled Oil, NBS, Gaithersburg, Maryland, November
29-30, 1977.
A-19 Yates, J. J., and K~. G. Croke. Used oil recycling in
Illinois Data Book. Prepared for the Illinois Institute of
Natural Resources by ETA Engineering, October 1978. Data
represents industrial samples obtained from Borg-Warner,
General Electric, Olin Brass, and John Deere.
A-20 Analytical data obtained from Tomas Leep, Water Quality
Division, Michigan Department of Natural Resources? analyse
performed over the period 1979 to 1981.
A-21 Analytical data obtained from Edgar J. Crowley, Division of
Air Quality, Minnesota Pollution Control Agency? date of
analysis 8-25-82.
A-22 Maney, J. P., N. Luedtke, and S. Drew. Hazardous waste
identification and listing support contract No. 68-01-6467,
delisting verification. Prepared by Energy Resources Co.,
Inc., for the U.S. Environmental Protection Agency. Sep-
tember 9, 1982.
A-154
-------
A-23 Massachusetts Department of Air Quality, Waste Oil Sampling
Program. Winter 1981/82, samples from facilities burning
waste oil.
A-24 Yates, J. J., and K. G. Croke. Used oil recycling in
Illinois Data Book. Prepared for the Illinois Institute of
Natural Resources by ETA Engineering, October 1978.
A-25 Swain, J. W. Industrial oils used as fuel. NBS Special
Publication 556. Proceedings; Workshop on Measurements and
Standards for Recycled Oil - II, Gaithersburg, Maryland,
November 29-30, 1977. p. 69.
A-26 Spawn, P. D., and P. F. Fennelly. An updated look at the
fuel potential of waste automotive oil. NBS Special Publi-
cation 556. Proceedings; Workshop on Measurements and
Standards for Recycled Oil - II, Gaithersburg, Maryland,
November 29-30, 1977. p. 51.
A-27 Linnard, R. E. Phillips recycled oil program. NBS Special
Publication 556. Proceedings; Workshop on Measurements and
Standards for Recycled Oil - II, Gaithersburg, Maryland,
November 29-30, 1977. p. 134.
A-28 Whisman, M. L., J. W. Goetzinger, and F. 0. Cotton. Waste
lubricating oil research. U.S. Bureau of Mines Pollution
RI 7925 (1974).
A-29 Skinner, D. J. Preliminary review of used oils in Canada.
Water Pollution Control Directorate. Report EPS 3-WP-74-4,
June 1974. Revised J,une 1976. p. 103.
A-30 Williams, B. R. Automotive crankcase drainings used for
fuel. NBS Special Publication 488. Proceedings; Workshop
on Measurements and Standards for Recycled Oil - II,
Gaithersburg, Maryland, November 22-23, 1976.
A-31 Unpublished data obtained from the Oklahoma Department of
Health; date of analysis: 9-4-80. Waste industrial oils to
be used for road base material.
A-32 Becker, D. A., and J. J. Comeford. Recycled oil program:
Phase I - test procedures for recycled oil used as burner
fuel. NBS Technical Note 1130, August 1980. p. 5.
A-33 Benz(a)pyrene concentration was given on page 51 of Refer-
ence A-32 for 11 used automotive oil samples and 8 used oil
samples taken from re-refiners' feedstocks. In ppm, the
automotive samples had concentrations of 10, 8, 11, 10, 11,
14, 14, 16, 12, 14, and 17; the re-refiners' feedstocks had
concentrations of 16, 10, 14, 13, 10, 14, 12, and 11.
0311
A-155
-------
A-34 Hazelwood, D. L., and F. J. Smith. Assessment of waste fuel
use in cement kilns. Prepared for Industrial Research Labo-
ratory, U.S. Environmental Protection Agency. March 1981.
A-35 Fu, T. T., and R. S. Chapler. Waste-oil boiler firing
demonstration at NAS Miramar, San Diego, California. Pre-
pared by Naval Civil Engineering Laboratory, Port Hueneme,
California. January 1982. p. 12.
A-36 Stringer, P. L. Correlation aspects of a virgin and a
re-refined engine oil containing the same additives. Pre-
sented at the NBS Conference on Measurements and Standards
for Recycled Oil - IV, September 12-16, 1982, Gaithersburg,
Maryland.
A-37 Weinstein, N. J. Waste oil recycling and disposal. Pre-
pared by Recon Systems, Inc., for the U.S. Environmental
Protection Agency. August 1974. p. 12.
A-38 Frame, E. A., and T. C. Bowen. U.S. Army/Environmental
Protection Agency re-refined engine oil program. AFLRL
Report No. 98, May 1978.
A-39 Unpublished analytical data obtained from the U.S. Environ-
mental Protection Agency; received 12-21-82. Data represent
automotive crankcase oil samples used as fuel.
A-40 Cheng, S. C., et al. Alternative treatment of organic
solvents and sludges from metal finishing operations.
Monsanto Research Corporation for the U.S. Environmental
Protection Agency. January 15, 1982. (Draft report.)
A-41 University of Wisconsin - Extension. Waste motor oil in
Wisconsin - A neglected resource. June 1976.
A-42 Unpublished data obtained from the U.S. Environmental Pro-
tection Agency; received 1-3-82. Data represent samples
taken from waste oil collectors in Connecticut. All oil
collected is assumed to be sold as fuel.
A-43 Unpublished composition data obtained from John R. Purvis,
New Jersey Department of Environmental Protection, September
3, 1982.
A-44 Unpublished composition data obtained from Wallace E.
Sonntag, Engineer with the New York State Department of
Environmental Conservation, January 11, 1983.
A-45 Unpublished composition data obtained from John R. Purvis,
New Jersey Department of Environmental Protection, January
7, 1983.
A-156
-------
A-46 GCA Corporation, "The Fate of Hazardous and Nonhazardous
Wastes in Used Oil Recycling," Fifth Quarterly Progress
Report, DOE DE-AC19-81BC10375, March 15, 1983.
A-47 Kansas City Star, Sunday, December 26, 1982 p. 25A.-
A-48 Unpublished analytical data developed for the Office of
Solid Waste, U.S. EPA by ERCO, 1983.
A-49 Unpublished analytical data developed by the National
Enforcement Investigation Center, U.S. EPA, 1983.
A-50 Ulrichson, D., and Yake, D. Iowa Re-refined Oil Fleet Test.
Engineering Research Institute, Iowa State University, Anies,
Iowa. October 1978.
A-157
0312
-------
-------
Appendix B
DATA BASE FOR
CONTAMINATION OF RESIDUES FROM
WASTE OIL PROCESSING AND RE-REFINING
0313
B-l
-------
TABLE B-l
METALS CONCENTRATIONS IN SETTLED SLUDGES
GENERATED DURING WASTE OIL STORAGE AND PROCESSING a/
Arsenic
<5
<5
<5
<1
<5
<5
<5
<5
r<5 b/
L 5 I/
<5
<5
r<5b/
L 17 c/
24 b/
<5 ~
<5
<5
<5
12
<5
12
14
<5
<5
5
r <5 b/
L <5 I/
0.013
<5
<5
<5
<5
<5
<5
<5
<5
<5
21
12
-
-
-
_
-
-
-
_
—
Barium
38
19
18
70
70
90
30
80
50
<10
47
4«
19
28
f 25 b/
L 1,950 c/
[1,200 b/
21 I/
3,610 c/
r 102 ¥/
L 385 I/
56 b/
310
420
<50
210
20
66
131
64
33
830
1.300
f 916 b/
L 1,140 c/
0.21
27
748
2,590
280
<50
<50
90
220
270
110
180
-
_
•
Cadmium
<0.5
<0.5
<0.5
<7
<7
<7
<7
r /
L <5 ^/
<5 b
<7
<7
<7
^10
^10
6
<5
<5
47
48
rso b/
L 47 c/
0.02
<8 •
148
11
*^10
*^10
^10
^10
<1Q
-------
TABLE B-2
TOTAL CHLORINE AND CHLORINATED SOLVENTS CONCENTRATIONS
IK SETTLED SLUDGES GENERATED DURING WASTE OIL STORAGE AND PROCESSING a/
Dichlorodifluoromethane
1.1.1-
Trichloroethylene
Trichloroethylene Tetrachloroethylene Total Chlorine
<1
<10
1.3
59
22
34
30
640
19
190
570
7,500
120
86
640
260
2,200
300
300
<100
1.200
<100 b/
110,000 b/
5,100 b/
420
9,900
790
5,400
<100
1,300
1,100
300
<100
500
400
200
<100
<100
<100
<200
2,300
-<200
240
<200
430
<100
770
2.2
5.7
1,300
360
37
110
370
730
600
100
<100
1,100
<100
900
1,100
<100 b/
900 b/
1,100 b/
<100
310
130
190
<100
<100
100
<100
<100
<100
<100
200
<100
<100
<100
<200
<200
<200
2.200
<200
<200
<100
<100
70
580
1,900
111
210
130
830
1.000
1.500
<100
1,600
1,000
1.500
<100
1.600
100 b/
1,400 b/
7.000 b/
740
210
200
210
<100
2.400
800
8,200
<100
<100
300
<100
<100
<100
<100
<200
<200
<200
<200
<200
<200
<100
<100
4,700
1.500
1.200
13,300
8,960
740
13.100
f 746 b/
I 2,940 c/
[2,530 b/
933 d/
1,880 c/
r 181,000 b/
I 75.400 c/
7,790 b/
2,910
3,630
88
2.390
1,300
5.080
2.540
13,600
220
1.860
1.540
1.470
2,110
593
1,270
851
1,780
1.300
<200
1,370
610
718
3,950
1,120
£/ All data are presented in ppm. No data were available on trichlorotrifluoroethane concentration.
b/ A top layer phase of an oily sludge residue.
c/ A bottom layer phase of an oily sludge residue.
~ZJ A middle layer phase of an oily sludge residue.
Note: Data for samples from different layers of the same storage tank are grouped.
Source: References B-24 to B-31.
0314
B-3
-------
TABLE B-3
OTHER ORGANICS CONCENTRATIONS
IN SETTLED SLUDGES GENERATED DURING
WASTE OIL STORAGE AND PROCESSING a/
PCBs Benzo(a)pyrene Phenol
1.4
<50 2.0 <1
<50 <1 <1
<50 <1 <1
<50 3.6 5.5
<10 12 11
<50 1.4 2.4
<4 16
28
<1
17
<1
<5
<10
500
<50
<50
<50
<50
<50
<50
<50
<50
<50
<50
<50
<2
<50
<50
a/ All data are presented in ppm. No data were available for the concen
tration of benzene, toluene, xylene, benzo(a)anthracene, or naphthale
Source: References B-24 to B-31.
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B-6
-------
TABLE B-6
OTHER ORGANICS CONCENTRATIONS IN WASTEWATER
GENERATED DURING WASTE OIL STORAGE AND PROCESSING a/
Benzene
<0.4*
<20*
550
38
24
150
890
290
300
669
Benzo(a)-
Toluene anthracene
14* <1*
1,300* <0.02*
840
120
2,500
530
5,800
640
630
693
Benzo(a)-
pyrene Naphthalene
<1* <1*
<0.02* 0.7*
ND b/
120
ND
700
470
ND
180
229
PCBs
<1*
<10*
<0.04*
14*
<0.04*
0.1*
<0.04*
<0.04*
<0.04*
<0.04*
<0.04*
Pheno:
65
<1*
0.02'
6,000
4,600
99,000
15,000
48,000
19,000
5,100
2,800
0.2*
<0.04*
<0.04*
0.04*
0.19*
<0.04*
ND
ND
ND
ND
ND
ND
ND
ND
ND
<10*
<10*
<5*
All data are reported in mg/£. unless coded by an (*) in which case the unit of measure-
ment is ppm. No samples were analyzed for xylene.
Not detected, however, no detection limit was reported.
irce: References B-20, B-22, B-24, B-26, B-27, and B-31.
031G
B-7
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-------
TABLE B-8
CONCENTRATION OF POTENTIALLY HAZARDOUS CONSTITUENTS
IN DISTILLATION BOTTOMS FROM RE-REFINING FACILITIES a/
Sample Number
etals
Arsenic
Barium
Cadmium
Chromium
Lead
Zinc
-
1,400
0
100
15,000
3,500
8.3
14
5.7
35
2,090
2,960
<0.01
25
20
7
1,090
126
1.0
6
9
11
4,235
85
15
940
29
63
10,300
133
hlorinated Solvents
Dichlorodifluoromethane - b/ - - - -
Trichlorotrifluoroethane - - - -
1,1,1-Trichloroethane -
Trichloroethylene -
Tetrachloroethylene -
Total Chlorine -
ther Organics
Benzene -
Toluene _----.
Xylene - - ' -
Benzo(a)anthracene - <4 - - -
Benzo(a)pyrene - <4 - - -
Naphthalene - - <4
PCBs - <11
eference B-7 B-22 B-26 B-26 B-26
/ All values are reported in ppm.
/ (-) indicates constituent was not measured. Generally, distillation bottoms are belie\
to contain very low levels of chlorinated and organic solvents.
0317
B-9
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-------
Appendix B
REFERENCES
B-l. Jervis, R.E. Trace Impurities in Canadian Oil Sands, Coals and
Petroleum Products and Their Fate During Extraction, Up-Grading,
and Combustion. Journal of Radioanalytical Chemistry, 71, No.
1-2. 1982. pp 225-241.
B-2. Unpublished data obtained by David William (U.S. EPA) from Steven T.
Cragg (American Petroleum Institute). August 19, 1982.
B-3. U.S. Environmental Protection Agency. Environmental Assessment of
Residual Oil Utilization - Second Annual Report. September 1978.
EPA 600/7-78-175.
B-4. Electric Power Research Institute. Study of Electrostatic Precipi-
tators Installed on On-Fired Boilers, Volume II. June 1978.
B-5. U.S. Environmental Protection Agency. Listing Waste Oil as a Hazardous
Waste. Report to Congress (SW-909). January 16, 1981.
B-6. Mascetti, G.J. and H.M. White. Utilization of Used Oil. Prepared for
the U.S. Department of Energy by the Aerospace Corporation. August
1978.
B-7. Becker, D.A., Editor. Measurements and Standards for Recycled Oil -
II. NBS Conference Proceedings, November 29-30, 1977.
B-8. Unpublished data obtained from John R. Purves, Office of Regulatory
Services, New Jersey Department of Environmental Protection. Jan-
uary 7, 1983.
B-9. Unpublished data obtained from Wallace E. Sonntag, New York State
Department of Environmental Conservation. January 11, 1983.
B-10. Hall, Robert R. Comparative Analysis of Contaminated Heating Oils.
Prepared for the U.S. Environmental Protection Agency by GCA Cor-
poration. May 1983.
B-ll. Unpublished data. U.S. Environmental Protection Agency Files. No
date.
B-12. Unpublished data received from Motor Oils Refining Company, McCook,
Illinois. No date.
B-13. Yen, T.F. The Role of Trace Metals in Petroleum. Ann Arbor Science
Publishers. Ann Arbor, Michigan. 1975.
0318
B-ll
-------
B-14. Valkovic, Vlado. Trace Elements in Petroleum. Petroleum Publishing
Company. 1980.
B-15. McCoy, J. The Inorganic Analysis of Petroleum. Chemical Publishing
Company. New York. 1962.
B-16. Proceedings of Symposium on Nonhydrocarbon Constituents of Petroleum.
Milwaukee, Wisconsin. March 30-April 3, 1952.
B-17. Bell, J.D. Recycling of Used Lubricating Oil as a Dust Suppressant,
Review of Current Knowledge and Recommendations for Further Investi-
gations. Prepared for the Petroleum Association for Conservation of
the Canadian Environment. December 1976.
B-18. Zobeli, C.E. Sources and Biodegradation of Carcinogenic Hydrocarbons
Proceedings of Joint Conference on Prevention and Control of Oil Pol-
lution. 1971.
B-19. Department of Energy. Motor Gasoline, Winter 1979-80. (DOE/BETC/
PPS-80/3). July 1980.
Residuals
B-20. Stoll, J.W. Wastewater Treatment System Design for the Re-refining
Industry. Proceedings of the Fourth International Conference on
Used Oil Recovery and Reuse. Association of Petroleum Re-refiners.
September 28-October 1, 1981.
B-21. Swain, J.W. Assessment of Industrial Hazardous Waste Management
Practices, Petroleum Re-refining Industry (SIC 2992). U.S. Environ-
mental Protection Agency. September 1976.
B-22. GCA Corporation. The Fate of Hazardous and Nonhazardous Wastes in
Used Oil Recycling. Prepared for Bartlesville Energy Technology
Center, Department of Energy. April 15, 1983.
B-23. Confidential data obtained by Franklin Associates, Ltd. included in
an environmental impact statement for a waste oil processing facili
Received March 1983.
B-24. Unpublished data obtained from John R. Purves, New Jersey Departmen
of Environmental Protection. September 3, 1982.
B-25. Unpublished data obtained from Don Hensh, Oklahoma State Department
of Health, November 4, 1982. Material is waste oil sludge mixed wi
rock used as a road base material.
B-26. Weinstein, K.D., T.D. Meyers, and S.R. Craft. Enhanced Utilizatiot
of Used Lubricating Oil Recycling Process By-Products. Prepared b}
Booz, Allen & Hamilton, Inc. for the U.S. Department of Energy (BE:
DOE/BC/10059-19. March 1982.
B-12
-------
B-27. Confidential data developed by the U.S. Environmental Protection
Agency, National Enforcement Investigations Center, obtained sum-
mer and fall, 1983.
B-28. Nims, J., et al. An Analysis of Waste Oil in Maine. Maine Depart-
ment of Environmental Protection. 1981.
B-29. Unpublished analytical data obtained from Henry Aho, Maine Depart-
ment of Environmental Protection. July 6, 1982.
B-30. Unpublished data obtained from the U.S. Environmental Protection
Agency; received 1-3-83. Data represent samples taken from waste
oil collectors in Connecticut.
B-31. U.S. Environmental Protection Agency. Data developed by ERGO for
the Waste Characterization Branch, Office of Solid Waste. Summer/
Fall 1983.
0319
B-13
-------
Appendix C
METHODOLOGY AND REFERENCES FOR USED OIL FLOW DESCRIPTION
The flow of used oil through the UOMS was developed for 1983
using information obtained from many sources and through making several
assumptions based upon the best available information. This appendix
provides the references and assumptions used to develop each number in
the overall flow description.
Figure C-l shows the actual flow of oil through the UOMS In
millions of gallons. The volumetric data has been removed in Figure C-2
and letter codes have been substituted. The references and assumptions
used to develop each number in the flow are described below for each
letter code.
It is important to note that the methodology which is used
accounts for oil flow only. Contaminants which accumulate in oil such
as water and solids are not included in the volumetric estimates. There-
fore, the actual quantity of material which is handled is greater, per-
haps by 10 percent, than the quantities shown.
(a) In 1983, a total of 1,251 million gallons of
automotive lubricants were sold in the United
States (C-12). About 94 percent of these
oils were crankcase or hydraulic oils which
comprise most of the oils generated following
use. According to information obtained from
(C-12), 42.1 percent of these oils were con-
sumed in passenger cars and 15.5 percent in
light trucks. Approximately 9.5 percent of
these oils were hydraulic fluids. Triple A
reports that 80 percent of passenger cars
and 54 percent of light trucks are privately
owned. For privately owned vehicles, a DOE
study indicated that 64 percent of all oil
changes are carried out by do-it-yourselfers
(DIYers) (C-l). Finally, oil generation
factors for passenger cars and light trucks
are 0.68 and 0.63, respectively (only 0.10
for hydraulic fluids). Using this informa-
tion, the total quantity of used oil generated
by DIYers is calculated below:
Passenger cars
Crankcase - [1,251 x (.94) x (.421) x (.80)
x (.64) x (.68)] = 155.2
Hydraulic oil - [1,251 x (.94) x (.421) x (.10)
x (.80) x (.64) x (.10)] - 2.5
Subtotal 157.7
c-i 0320
FRANKLIN ASSOCIATES, LTD.
-------
1
«r
i t
o
c
a
a
0
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C
c
I.
3
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m
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i
sg
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192.3 million gal
use In on- site bo
bases, used oil p
I «/t t/i >>
i!.^
'o u —
Iff1
C-2
-------
0321"
C-3
-------
Light Trucks
Craakcase - [1.251 x (.94) x (.155) x (.90)
x (.54) x (.64) x (.63) - 35.6
Hydraulic Oil - [1,251 x (.94) x (.155) x (.10)
x(.54) x (.64) x (.10) -
Subtotal
Total DIYer Oil 193.9
(b) The management of used oil generated by DIYers was assumed
to be equal to the average practices reported by DOE for
conditions in 1981 (C-l). Volumes managed in each way were
calculated from total generation using the following per-
centages:
Take to recycle center - 14.0 (27.1 mil gal)
Disposal - 21.0 (40.8 mil gal)
Dumping - 60.9 (118.0 mil gal)
Burning - 4.1 (8.0 mil gal)
100.0
(c) The total quantity of used oil generated at "automotive
generators" (see definition in Section 2.0) was calculated
based upon sales to certain markets. These markets include
personal and commercial vehicles with commercial being
either fleet or non-fleet. The generation by non-DIYer
personal vehicles can be calculated by using the same
method and equations as presented above for DIYers.
Oil generation by non-DIYer personal vehicles is about
55 percent of that generated by DIYers. or 106.8 million
gallons. Oil generation by commercial vehicles is cal-
culated below based upon sales (C-12) and generation
factors (C-.2) and (C-12) for three basic markets and
two general oil types.
, (Generation (Used Oil
(Sales - 10 gal) x Factor) - Generati
Passenger Cars
Crankcase (86.8)
Hydraulic (9.6)
Light Trucks
Crankcase (72.0)
•Hydraulic (8.0)
Medium & Heavy Trucks & Buses
Crankcase (139.7)
Hydraulic ( 15.7)
x (0.68)
x (0.10)
Subtotal
x (0.63)
x (0.10)
Subtotal
x (0.59)
x (0.10)
Subtotal
60.0
82.42
1.57
84.0
Total - Commercial Vehicles 190.2
C-4
FRANKLIN ASSOCIATE
-------
The remaining automotive used oil generation results
from off-road engines including such uses as farming, con-
struction, mining, military, and aviation. Both crankcase
and hydraulic oil sales (C-12) and generation factors (C-2)
and (C-12) were used to calculate used oil generation in
these markets as shown below.
Off-Road Market
Farming
Crankcase
Hydraulic
, (Generation
(sales - 10 gal) x Factor) •
(Used Oil
Generation;
(74.1)
(39.7)
x (0.59)
x (0.75)
Subtotal
Construction
Crankcase
Hydraulic
(68.8)
(34.7)
x (0.59)
x (0.75)
Subtotal
Mining
Crankcase
Hydraulic
(45.5)
(23.1)
x (0.59)
x (0.75)
Subtotal
Government
Crankcase
Hydraulic
(11.7)
( 6.3)
x (0.63)
x (0.75)
Subtotal
Aviation
Crankcase
Hydraulic
(12.7)
( 7.6)
x (0.47)
x (0.75)
Subtotal
Total - Off-Road Vehicles 208.1
The total volume of oil accumulated at automotive
generators equals the sum of the following components:
Oil received from DIYers -
Non-DIYer personal vehicles -
Commercial on-road vehicles -
Off-road vehicles -
Total
27.1 mil gal
106.8 mil gal
190.2 mil gal
208.1 mil gal
532.2 mil gal
C-5
FRANKLIN ASSOCIATES, LTD.
-------
(d) The letter "d" codes represent outputs from automotive
generators.
(dl) - Some automotive oils are generated by industrial
establishments due to the use of vehicle fleets.
This quantity was estimated assuming that 8 per-
cent of the oil generated by medium and heavy
trucks and buses is in industry fleets. This
percent is equal to the percent of total fleets
comprised by the manufacturing process and
petroleum industries (C-13).
(d2) - Automotive generators use their oil as fuel in
three major applications: (1) waste oil heaters;
(2) diesel engines; and (3) on-site boilers.
Some minor burning may take place in other fuel
applications, but that activity is not included
in this estimate.
Used oil heaters burn primarily automotive oils.
They are usually located at automotive generator
sites. It has been estimated that about 30,000
heaters are currently in use in the United States
with a typical rating of about 250,000 Btu/hour
(C-4). Based upon this rating and other information
received from industrial contacts, it was assumed
that a typical unit would burn 1,140 gallons per
year. The total quantity of used oil burned in this
way is estimated to be 34.2 million gallons in 1983.
Little documented information is available on used
oil combustion in diesel engines. Some large diesel
engine manufacturers, such as Cummins, have provided
customers with instructions and apparatus for blend-
ing used diesel oil with diesel fuel for burning in
diesel engines. The blending ratio is about 50 to
1 (fuel to oil). It is estimated that only 10 to
20 million gallons of the 200 plus million gallons
of truck oil is burned in this way. The midpoint
of 15 million gallons per year was assumed for this
study.
Burning of automotive oils in on-site boilers is
primarily limited to the U.S. Department of Defense
Approximately 50 percent of total generation by U.S
government installations (6.0 million gallons!, is
estimated to be burned on-site (C-14).
Overall. 55.2 million gallons (34.2 + 15 + 6.0)
of generated used automotive oil is estimated to be
burned directly by generators.
C-6
FRANKLIN ASSOCIATE
-------
(d3) - It was assumed that 20 percent of the used oil
generated by the farming, construction, and mining
industries which was not collected into the UOMS
was used to oil roads or other unpaved areas to
suppress dust or to provide an asphaltic effect
to the surface. Total non-collected generation
for these sectors was 125.3 million gallons in
1983. This volume equals 80 percent of farm
generation and 60 percent of construction and
mining generation. Twenty percent of this volume
equals 25.1 million gallons?
(d4) - Some generated used oil is dumped by non-fleet
commercial vehicle operators and a substantial
volume is dumped by operators of off-road vehicles.
Most dumping is simply allowing oil to drain from
a crankcase onto an unpaved lot or road; however,
it is sometimes collected and used in a haphazard
manner for other purposes such as weed or insect
control. It was assumed that 12.5 percent of all
oil generated by commercial vehicles is dumped.
This practice is only common for small non-fleet
situations where the volume of oil generated is
too small to warrant storage with subsequent col-
lection. The 12.5 percent estimate assumes 50
percent of the commercial vehicle oil generation
is for non-fleet vehicles (91.8 million gallons);
50 percent of that oil is not collected into the
TOMS (45.9 million gallons); and 50 percent of the
non-collected generation is dumped (22.9 million
gallons).
As stated in the preceding section, 125.3 million
gallons of used oil generated by the farming, con-
struction, and mining industries is not collected
into the UOMS. Of this total, 80 percent (or 100.2
million gallons) is believed to be dumped.
Overall, 123.2 million gallons of used automotive
oil is estimated to be dumped by generators, not
including DIYers.
(d5) - Only a small amount of generated used automotive
oil is believed to be disposed of through conven-
tional methods (e.g., sanitary landfill). It was
estimated that 10 percent of the non-collected, non-
fleet, commercial vehicle oil was managed in this
way:
Disposed oil - (45.9 mil gal) x (.10) » 4.6 mil gal
C-7
0321
FRANKLIN ASSOCIATES, LTD.
-------
(e) Total used oil generation by industrial establishments
was determined based upon sales reported in (C-12) and
generation factors reported in (C-2) and (C-8) with some
adjustments by FAL. Table C-l summarizes this calculation
procedure. Note that actual generation (shown in parenthe-
sis for some oils) is lower than the theoretical volumes
calculated from the factors. This is because some oils
which are sold do not complete their life cycle in the
year in which they are sold. In effect, there are more
of these oils in use each year.
(f) Used oil management practices by industrial facilities
was estimated by determining generation by major industrial
sectors and applying survey results on average management
methods to the volume for each sector. Table C-2 shows
industrial oil generation in 1983 by the major sectors.
Table C-3 shows estimates of how the generated oils are
managed in each major sector.
(g) The total oil entering the UOMS is the sum of that supplied
by automotive generators and industrial generators. Oil
entering UOMS - 317.4 + 351.7 - 669.1 mil gal.
(h) Although many independent collector companies exist, it
was assumed that they only collect 25 percent of the oil
accumulated by generators. The remaining 75 percent is
collected by processors and re-refiners. This 25/75 per-
cent breakdown was estimated based upon collection prac-
tices in many geographical regions as reported by col-
lectors and processors. These percentages were applied
to the total oil entering the UOMS to give the volume
handled by independent collectors and the volume collected
directly by processors and re-refiners.
Ind. Collectors - (669.1) x (.25) - 167.3 mil gal
Direct Collection
by Proc. and
Re-ref - (669.1) x (.75) - 501.8 mil gal
(i) The distribution of oil from independent collectors
companies was estimated based upon telephone interviews
and site visits with collectors and processors. Approxi-
mately 62 percent of the collected oil is delivered to
processors or re-refiners. The remainder is sold directly
to end-use applications including road oiling (14%), direc
fuel sales (9.5%), and virgin fuel oil dealers (9.5%), or
lost to disposal (5%).
C-8
FRANKLIN ASSOCIATE
-------
Table C-l
1983 INDUSTRIAL OIL SALES/GENERATION
UO6 gal)
Sales x Generation Factor I/
I. General Industrial Oils
A. Hydraulic
B. Gear
C. Other Specified
1. Turbine Circ.
2. Refrigeration
3. Way
A. Compressor
5. Rock Drill Air Tools
D. Other
Subtotal
II. Industrial Engine Oils
A. Railroad Diesel
B. Marine
C. Natural Gas
Subtotal
III. Metalworking Oils
A. Metal Removing
B. Metal Forming
C. Metal Treating
D. Metal Protecting
Subtotal
IV.
Process Oils
A. Elecmcal
B. White
C. Rubber
D. Other
Subtotal
INDUSTRIAL GREASE
TOTAL INDUSTRIAL LUBRICANTS
VI. Industry Fleet Oils
A. Automotive Oil
TOTAL OIL GENERATION BY INDUSTRIAL GENERATORS
264
33
78
6
5
4
3
28
421
57
49
38
144
85
47
19
12
163
76
56
64
102
298
1,026
35
1,061
11.2
.80
.60
.60
.33
.60
.60
.60
.73
.20
.50
.20
1.00
0.60
0.60
0.10
.90
.10
.10
.10
55.3
0
53.5
Generation
211.2 (200) 21
20.0 (19.6)
(295.1)
11.4
24.5
7.6
85.0
28.2
11.4
1.2
125.8
68.4 (20.5) 3/
5.6
6.4
10.2
90.6 (42.7)
567.6 (507.1)
0
567.6 (507.1)
_!/ Generator factor equals the fraction available for collection into the used oil management system;
it does not include oil which ends up in wastewater treatment sludges generated on-site.
y Values in parentheses equal actual industrial oil generation Assuming that all oil sold in any one
~ year does not finish its life cycle in that same year. Thus, there is an accumulation of oil in
use in our industrial/conmercial system.
_3/ The relatively low level of actual used electrical oil generation is due to the fact that much of
~ electrical oil sales are to replace PCB oils in transformers. The generation of these PCB oils is
not included in this value since these oils do not enter the UOMS.
Source: Sales data: (C-12).
Generation factors: (C-2) and (C-8) and Franklin Associates, Ltd.
C-9
0323
-------
Table C-2
INDUSTRIAL OIL GENERATION - 1983
Number of Establishments
SIC
Major Generators
Less than
20
Employees
24 Wood Products 29,032
25 Furniture & Fixtures 6,128
26* I/ Pulp/Paper 72
27* Newspapers 7,745
28 Chemicals 2.179
30* Rubber/Plastic 6,673
31* Leather 206
32* Glass 237
33 Primary Metals 3,687
34 Fabricated Metals 20,985
35 Machinery 39,784
36 Electronics 9,785
37 Motor Vehicles 5,656
38 Instruments 5,145
39 Miscellaneous Manufacture 12,210
49* Electric Utilities -
Subtotal - Major Generators 149,524
All Other Mfg. Industries
Marine Terminals
Military
Commercial
Railroads
Sia^ior.ary Natural Gas Engines
Other Miscellaneous Uses _5/ •*
Total Industrial Oil
Greater
than 20
Employees
Used Oil Generation
(103 gallons)
Total
Small
facilities
Large
Facilities
Total
5,451
3,450
548
2,475
1.880
5,127
170
228
3,966
12,791
14,234
7,329
3,430
1,988
3,556
1,068 2/
67,721
34,483
9,608
620
10,220
4.059
11,800
376
465
7,653
33,776
54,018
17, 114
9,086
7,133
15.766
1,068
217,245
2.908.7
135.0
30.1
US. 5
1,663.0
1.315.1
16.4
42.0
4.425.0
3,725.0
9,780.0
1.314.5
7,486.8
86.6
2,613.4
-
35,660.1
4,166.2
506.8
7,996.8
308.9
24.627.8
6,113.5
85.9
1.206.7
66,329.1
16.886.4
41,812.6
20,775.6
143,885.0
1.124.9
3,101.4
13,243.2
352,170.8
7.074.9
641.8
8.026.9
427.4
26.290.8
7,428.6
102.3
1.248. 7
70,754.5
20.611.4
51,592.6
22,090.1
151,371.8
1,211.4
5,714.8
13,243.2
387,830.9
140.000
153
153
NA.3/ -
NA
NA.
306
36.663.1
306
20,000 4?
11,400
7,600
50,000
513,800
I/*: The entire industry is not included in the major generator analysis because of a lack of data or be
~ segments are insignificant generators.
2/ All power plants in SIC 49 are assumed to satisfy the large establishment definition of >20 employe
_3/ NA: Not Available.
-•_, Estimated from the total generation believed to be 24 million gallons.
5_/ Includes such things as the use of industrial oils in homes, commercial establishments, off-road
~ vehicles, etc.
Source: Franklin Associates, Ltd., from data provided in (C-9) to (C-ll) and (C-15).
C-10
-------
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0325
-------
(j) The total volume of used oil handled by reprocessors
and re-refiners is equal to the sume of that delivered
by independent collector companies (103.4 million
gallons) and that which is directly collected by pro-
cessor and re-refiner route trucks (501.8 million gal-
lons). The total input to these companies equals the
sum of these numbers or 605.2 million gallons.
(k) The distribution of collected used oil to the eight
selected model facilities is based upon several as-
sumptions. First, it should be emphasized that there
are actually many more types of facilities than the
selected typical models, and therefore, the total
volume of oil was "force fed" to a workable number of
facilities.
Three basic data sources were used to estimate oil
distribution to the typical models—(1) the volume
handled per year by each model, (2) the total number
of processing and re-refining companies, and (3) the
total volume of oil delivered to these companies.
It has been reported that there are approximately 250
operating processors and re-refiners in the United
States (C-5). Some information is available through
limited surveys as to the number of specific company
types. Good information is available characterizing
the relatively small number of operating re-refiners.
Using available information, a series of iterations
was performed to determine a reasonable number of
facility types while maintaining the desired volume
of material throughput. Table C-4 shows the results
of those iterations and the estimated flows. The data
in Table C-4 are presented in two basic parts; one part
consisting of the first four columns and the second
part, the last column. The first part develops the
total annual volume and percent of oil passing through
each selected model type. The resultant estimates
yield a total volume which is greater than the actual
input to the model facilities (663 compared to 605.2
million gallons). This exercise was carried out to
determine the percentages shown in column four which
could be applied to the total input to processor
companies to give material flows into each model which
are consistent with the overall flow description. These
percentages were multiplied times the remaining input
material after the re-refiner volume of 85 million gal-
lons had been subtracted. This independent estimate of
re-refining was maintained because considerably more
information was available about this entire industry.
C-12
FRANKLIN ASSOCIATE:
-------
Table C-4
DEVELOPMENT OF BEST ESTIMATES OF USED OIL DISTRIBUTION HTTP PROCESSING ASP RE-REFINING MODELS
Model Facility
Minor Processors
MP-1
MP-2
Major Processors
MJP-1
MJP-2
MJP-3
MJP-4
Subcocal - Processing
Re-Refiners
RR-lt
RR-2f
Subtotal - Re-refining
Total
Number
of
Facilities
50
65
60
20
20
25_
240
3
12
13
253
Model
Facility
Annual
Volume
(1Q3 gal)
750
1,500
2.500
2.500
2.500
7,500
3.500
8,000
.
Total
Annual
Volume
(106 gal)
37.5
97.5
150.0
50.0
50.0
187.5
572.5
10.5
80.0
90.5
663.0*
Percent
of
Total
Processed
Oil
6.6
17.0
26.2
8.7
8.7
32.8
100.0
-
-
Estimated
Oil . ,
Handled by
Each Mode It
34.3
88.4
136.3 (139.4)**
45.3 (46.3)**
45.3 (46.3)**
170.6 _(1?4.7)**
520.2 (529.4)**
10
21
85
605.2 (614.4)**
This value is greater than the total estimated volume of material handled by processors and
re-refiners (605.2 mil gal). Some disagreement is expected because the total annual volume
was calculated based upon typical facility volumes rather than average volumes. Since the
actual number of facilities was factored with typical volumes, agreement in total volume
would be mere coincidence.
t The number of re-refining facilities and volumes of oil handled were independently estimated
and held fairly constant in this analysis because a high level of confidence exists in those
estimates.
J The estimated volumes passing through the processor models were calculated to fit the oil volume
which remained following the subtraction of the re-refiner estimates. For example, the oil flow
through MP-1 was calculated by:
(520.2) x 0.066" 34.3 million gallons.
** The volumes shown in parentheses for major processors and re-refiners are adjustments associated
with oil received from minor processors. In effect, this is double counting. Although only
605.2 million gallons enter the system, 614.4 million gallons are actually handled because of
inter-facility transfers. See code (1) for a description of minor processor oil distribution
practices.
C-13
032G
-------
Adjustments in the volume of oil handled by each major
processor type (Kls) is shown in Table C-4 in parentheses.
These adjustments represent oil which passes from minor
processors to major processors as part of normal flows
(see letter codes "1" and "m"). Therefore, the actual
volume of oil handled is somewhat higher than the amount
entering the UOMS.
(1) The distribution of product oil from the selected pro-
cessing and re-refining model facilities is based upon
the results of a limited survey of companies. Table C-5
summarizes the percent distribution of product oil from
processors, re-refiners, and independent collectors.
These estimates were taken directly from the detailed
market analyses developed for each model facility.
Also, included in Table C-5 is the calculated distribu-
tion of all input oil including product oil and oil losses
and disposal in processing residues. Since residue gen-
eration and disposal practices vary tremendously for
different facility types, it was estimated that a 5 per- .
cent loss factor is common for processing facilities.
The disposal estimates shown for re-refiners is greater and
based upon reported practices as obtained in the company
survey. The output gallonage for each model was calcu-
lated from the percentages shown in Table C-5 and the
estimated input to the facilities (k).
(m) The amount of used oil handled "twice" by the UOMS (once
by minor processors and once by major processors or re-
refiners) was calculated from the outputs from the two
minor processors models classified as the "major proces-
sor/re-refiner" market.
(MP-1) - 4.8 mil gal
+(MP-2) - 4.4 mil gal
Total 9.2 mil gal
(n) Total re-refined lube oil is equal to the sum of lube oil
produced by the acid-clay and vacuum distillation re-re-
finer models.
(o) Non-fuel industrial uses for product oil includes flo-
tation oil for the phosphate industry, and material
feedstock for asphalt manufacture, and form oil. The
total oil consumed for this purpose is the non-fuel
industrial output from the processor models and the
bottoms material produced by vacuum distillation
re-refiners.
C-14
FRANKLIN ASSOCIATE
-------
Table C-5
SUMMARY OF USED OIL DISTRIBUTION FROM MODEL FACILITIES*
(percent)
Virgin Other
Direct Oil Processors
Fuel Fuel Non-Fuel Road or
Model Facility Sales Dealer Industrial Oiling Re-refiners
Collector Only 9.5Z 9.5Z - 147 62Z
Minor Processors
MP-1
Product Oil 25 45 5 10 15
Total Oil Input 24 43 5 9 14
MP-2
Product Oil 30 50 5 5 5
Total Oil Input 28 47 5 5 5
Major Processors
MJP-1 and MJP-2
Product Oil 45 40 8 2 -
Total Oil Input 43 38 7 2 -
MJP-3 and MJP-4
Product Oil 60 30 3 2 -
Total Oil Input 57 28 3 2 -
Re-Refiners
RR-1 _____
RR-2 - 12 -
On-Site
Fuel
-
-
5
5
5
5
5
5
n
n
Lube Oil Disposal Total}
65
75
5Z
28
6
100
100
100
100
100
100
100
100
100
100
100
* Used oil distribution is described as the percent of total oil output. For the processor models, two sets
of percentages are shown. The first shows product oil distribution only; the second is based upon total
oil input and includes oil losses in disposal residues.
t Sum of calculated percents as related to total oil input may not equal 100 due to rounding.
J It was assumed that the recovered distillate fuels are burned in-house for process heating.
Source: Franklin Associates. Ltd., from a limited survey of facilities including site visits (C-15).
C-15
0327
-------
(p) Total used oil sales through virgin oil fuel dealers
was calculated as the flume of V.O.F.D. outputs from
the processor and Independent collector models.
(q) Total burned used oil equals the sum of (1) burning
by DIYers, (2) fuel use by generators, (3) fuel sales
by all processors and collectors, (4) V.O.F.D. sales,
(5) distillate fuel production by re-refiners, and
(6) on-site burning by processors.
(r) The estimate of the volume of used oil burned In large
and small boilers was calculated as the difference in
the total oil burned and the sum of oil burned in cement
kilns, diesel engines, space heaters, and on-site boilers.
(s) Cement companies routinely burn waste materials along
with conventional fuels to provide the large .amounts
of heat required for cement kiln operation. The pub-
lished fuel statistics for this industry do not dis-
tinguish between u iste fuels consumed which include
used oils, solvents, and contaminated fuel oils (C-6).
The Portland Cement Association reports that used oil use
is not significant, but some may .be used with consumption
ranging from 0 to 10 million gallons per year (C-7). For
this study, the midpoint volume of 5 million gallons per
year was ae°imifi'^r
(t) and (u) Used oil burned in diesel engines and space
heaters was previously evaluated in the letter (d)
discussion which examined generator used oil use as
a fuel.
(v) Processors and re-refiners burn used oil and light dis-
tillates recovered through processing to provide on-site
process heat and sometimes space heat for buildings. From
the processor survey, it was estimated that approximately
3 percent of product oil is burned on-site. Re-refiners
often burn the recovered distillate fuels which comprise
about 7 percent of input used oil (C-ll). In total,
on-site burning by processors and re-refiners was esti-
mated to be 30.7 million gallons in 1983.
Also included in the on-site boiler use -is burning by
industrial facilities (see letter "f" - 37.1 million
gallons) and the burning of primarily automotive oils
by military bases (see letter "d2" - 6.1 minion gallons).
Overall, a total of 73.9 m-tlljon gallons were believed to
be burned in on-site boilers In 1983.
C-16
PRANKUN ASSOCIATES
-------
(w) Total road oiling was estimated by summing the road
oiling activity of each processor model, the inde-
pendent collector model, and in-house generator usage.
(x) and (y) Used oil disposal primarily includes the con-
ventional techniques of landfilling and incineration
and the undesirable method of dumping. Some oil may
enter into disposal lagoons or the municipal sewer.
systems, but overall, these avenues of disposal are
believed to be of minor significance. For this analysis,
it is not possible to totally distinguish between land-
filling and incineration methods; however, industrial
oils are about 5 times more likely to be land disposed
than incinerated (see Table C-3).
Some oil is disposed of at every stage in the UOMS.
The DIYer may put the oil in the municipal solid waste
stream; the industrial generator may have a private
hauler dispose of a highly contaminated used oil; and
processors and re-refiners produce sludges with variable
oil contents for disposal. The (x) value is the sum of
these disposal estimates for each selected UOMS model,
as well as the generators.
Used oil which is dumped (letter "y") originates from two
basic sources: (1) DIYers and (2) off-road vehicle oper-
ators. According to the DOE DIYer study (C-l), about 60
percent of the oil generated by DIYers is dumped. The
dumping of oil generated by off-road vehicles has been
previously discussed in the generator use disposal
section (d4).
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APPENDIX C REFERENCES
C-l Gottlieb, J., "Analysis of Potential Used Oil Recovery from Individ-
uals," DOE/BC/10053-21, 1981.
C-2 Weinstein, N. J., "Waste Oil Recycling and Disposal," Recon Systems,
Inc., for the U.S. Environmental Protection Agency, August 1974.
C-3 Resource Technology, Inc., RTI Newsletter, 1982.
C-4 Development Planning and Research Associates, Inc., "Selected Charac
teristics of the Waste Oil Space Heater Industry." EPA Contract No.
68-02-3173, July 1983.
C-5 Development Planning and Research Associates, Inc., "Interim Report
for the RCRA Economic Impact Analysis of the Effects of the Waste
Oil Regulations on the Waste Oil Management System—System Descrip-
tion." EPA Contract No. 68-01-6322, May 1981.
C-6 Portland Cement Association, Energy Report, U.S. Portland Cement
Industry, August 1982.
C-7 Personal communications with Rob Roy, Portland Cement Association,
October 20, 1982.
C-8 Richard J. Bigda & Associates, "Review of All Lubricants Used in
the U.S. and Their Re-refining Potential," prepared for the Bartles
vill Energy Technology Center, U.S. DOE, June 1980.
C-9 U.S. Department of.Commerce, Bureau of Census, Census of Manufactui
1977 and 1982.
C-10 U.S. Department of Commerce, Bureau of Industrial Economics, 1984
U.S. Industrial Outlook.
C-ll U.S. EPA, "EPA Survey of Handlers and Burners of Used or Waste Oil
and Waste-Derived Fuel Material," survey performed 1983-1984, data
obtained from computer files.
C-12 Brecht, F., "Outlook for U.S. Lube Oil Supply and Demand," present
at the 1983 National Petroleum Refiners Association Annual Meeting
by Pennzoil Products Company, March 20-22, 1983, San Francisco.
C-13 1981 Commercial Car Journal Fleet Census.
C-18
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C-14 Fu, T. T., and C. Semien, "Utilization of Navy-Generated Waste Oils
as Boiler Fuel - Handbook of Guidelines and Field Survey Results,"
Naval Civil Engineering Lab, Port Hueneme, California, August 1983.
C-15 Franklin Associates, Ltd., survey of selected industries and site
visits to industrial establishments to assess used oil generation
and management practices, information obtained May 1983 to August
1984.
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Appendix D
ALTERNATIVE METHOD TO CALCULATE MEAN CONCENTRATION
OF HAZARDOUS CONSTITUENTS IN USED OIL
There was some question among the research team and the U.S. EPA
regarding the most appropriate method to calculate the mean concentration
of hazardous constituents. Throughout this report mean concentrations
are presented for detected concentrations only. Non-detected values vere
not included in those calculations because detection limits varied signif-
icantly. For example, many PCS tests had a detection limit of 50 ppm, but
others could measure concentrations down to 1.0 ppm. It seemed inappropriate
to consider samples with levels of <50 ppm and <1 ppm equal to zero, or even
equal to their detection limits. There seemed to be no single method which
would avoid distortion. That is why means were calculated for detected
values only throughout this report.
Nevertheless, some individuals believed that the conservative
approach of assuming the concentration to be equal to the detection limit
to be the most appropriate for some risk assessment calculations. For this
reason, an alternative mean was calculated for each contaminant for most
used oil types. Table D-l shows these values assuming that the concentration
of the contaminant in a non-detected situation was equal to the detection
limit (e.g., <50 « 50; <1 - 1).
D-l
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