United States
                                   Environmental Protection
                                   Agency
                                   Health Effects Research
                                   Laboratory
                                   Cincinnati OH 45268
V-/EPA
                                   Research and Development
                                   EPA-600/S1-81-063  Feb. 1982
Project  Summary
                                   Mechanisms of Cadmium
                                   Absorption  in   Rats

                                   E. C. Foulkes, D. R. Johnson,  N. Sugawara, R. F. Bonewitz, and C. Voner
                                     This study was undertaken in order
                                   to help  clarify the factors which
                                   determine the fractional absorption of
                                   an oral load of cadmium (Cd) from the
                                   intestine of the rat. The experiments
                                   utilized intact segments of intestine,
                                   perfused or incubated in situ with their
                                   blood supply intact. Absorption of Cd
                                   from the jejuna! lumen can be ascribed
                                   to a saturable membrane system; that
                                   is, after  short periods of exposure
                                   essentially all the metal removed from
                                   the lumen was recovered in mucosal
                                   tissue  (Step I). The second step in Cd
                                   absorption, i.e., transfer of the metal
                                   from mucosa into blood, proceeded at
                                   only 1 -2% of the rate of uptake from
                                   the lumen (Step I).  No  evidence was
                                   obtained for a role of metallothionein
                                   in the mucosal retention of Cd. Step I
                                   of Cd  absorption was inhibited by a
                                   variety of exogenous and endogenous
                                   factors.  Thus, zinc was  found  to
                                   depress Cd transport in  an apparently
                                   competitive manner. Addition of milk
                                   to the  lumen also inhibited Cd uptake,
                                   an effect entirely due to the Ca
                                   content.  Bile salts act as endogenous
                                   modulators of  Cd  absorption; their
                                   effect may be related to micelle
                                   formation.
                                     The  research also included  studies
                                   of duodenal and ileal Cd transport.
                                   Heal Cd absorption differed from that
                                   in the jejunum by a relatively much
                                   faster  Step II. Unlike the low ratio of
                                   Steps  ll/l for the toxic metal in the
                                   jejunum, the ratio  for  the essential
                                   metals Cu and Zn was much higher
                                   (about 50%). Absorption of Cd by the
                                   gut in neonatal rats proceeds much
                                   faster than in adults; reasons for this
                                   difference have not yet been clarified.
                                   Another question remaining under
                                   study is the extent to which different
                                   metals  such as Cd  and  Zn share
                                   common absorptive mechanisms.
                                     This Project Summary was devel-
                                   oped by EPA's Health Effects Research
                                   Laboratory, Cincinnati, OH, to an-
                                   nounce key findings of the research
                                   project that is fully documented in a
                                   separate report of the same title (see
                                   Project Report ordering information at
                                   back).

                                   Introduction
                                     The human environment contains a
                                   variety of heavy metals, originating from
                                   both natural and anthropogenic sources.
                                   Some of these metals are  clearly
                                   essential  for life, while for some others
                                   a biological function has been sug-
                                   gested. However,  many of these ele-
                                   ments,  in  the form  of organic  or
                                   inorganic compounds, are highly toxic.
                                   The level of such  compounds in the
                                   environment may therefore bear directly
                                   on human  health. Analysis of their
                                   effects assumes  additional urgency
                                   because of the likelihood that ambient
                                   concentrations of these metals may be
                                   increasing.
                                     A special problem in this regard is
                                   posed by cadmium. Significant amounts
                                   of this element are being added to the
                                   environment through use  of  sewage
                                   sludges  and other fertilizers on agri-
                                   cultural land, from combustion of fossil
                                   fuels, and  by other processes The

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problem is exacerbated by the fact that
the half  life  of  Cd in the body, and
especially the kidneys, is very long; in
effect, Cd acts as a cumulative poison.
Its prime target organ is the kidney, and
nephropathy has been reported  in
exposed human populations.
  Main  sources  of the  human body
burden of Cd outside of occupational
environments are Cd  in food  and
tobacco smoke. The non-smoker derives
most of his Cd through gastrointestinal
absorption. In spite of this fact, relatively
little is  known about mechanisms  of
intestinal Cd absorption, and about the
factors which on the whole reduce net
fractional absorption to  only a  few
percent of the oral load. This considera-
tion defined the objective of the research
descirbed in  this report. A scientific
interest  in the  basic  mechanism  of
metal transport,  and the possibility of
applying knowledge gained to the
control of metal absorption, formed the
starting points.
  Throughout the work attempts were
made to follow  absorption under as
physiological  conditions as possible,
using isolated segments of intestine in
situ in the living animal. No attempt was
made to repeat in detail material already
published. Copies of papers and abstracts
based on these results are appended to
the report. These papers  should be
consulted for  details.


Results
  The results reported  here extend
earlier work  by  other  investigators.
However, unlike several of these
investigators,  the present findings were
made with intact intestinal segments in
situ at Cd  concentrations  one might
conceivably encounter in heavily polluted
areas.  Previous  work in many cases
used excessively high Cd  concentra-
tions. In  addition, the preferred tech-
niques  often were the analysis  of
absorption in  the intact  animal, or the
measurement of  transport  by everted
sacs of intestine  in vitro. In both cases,
the avid retention of Cd in the intestinal
wall was a source of difficulty.
  Thus, in sacs, cadmium is not likely to
diffuse across the submucosal tissues
into  serosal  fluid as  readily as, for
instance, sugars  or amino acids. There-
fore, the release of Cd from mucosa in
sacs may differ quantitatively from that
occurring under physiological condi-
tions. Also, in the intact animal entero-
hepatic recirculation makes it impossible
to obtain  absolute  values  for the
unidirectional  movement of Cd from
lumen into mucosa and blood.  The
method employed in this study proved a
more appropriate procedure for the
detailed analysis of Cd absorption under
reasonably physiological conditions.
  From results obtained the following
conclusions may be drawn:
  (1)  Cd is removed from the lumen of
      the rat jejunum by a membrane-
      related process which  exhibits
      saturation kinetics (Step I). After
      short periods, essentially  all Cd
      thus  removed can be recovered
      from the mucosa. An activity
      gradient exists along the jejunum.
  (2)  Step I or Cd transport is modulated
      by bile salts as well as by a  variety
      of food constituents.
  (3)  Zinc   interacts  in an apparently
      competitive  manner with  Cd for
      transport by Step I (Figure  1). The
      inhibitory effect of Zn  on  Cd
      uptake is  illustrated in  Figure  2,
      using  more conventional  units.
      Unlike Cd,  however, Zn  is not
     appreciably retained in the  muco-
     sa. In spite of the competition for
     Step I, the transmural movement
     of Zn and Cd is not mediated by
      identical mechanisms.
  1.8-
•  7.2H
So. 6-
 00
-2?
 o
  0.4-
                Zn 5.0 mM,
10
20
                  30  40  50
                Cd
 Figure  1.     Effect of Zn and Cd up-
              take. Cd was transported
              out of the lumen at a con-
              stand exponential rate for
              30 mm. from  which the
              mean initial rate (M±SE)
              of transport was calculated
              in nmole Cd/g tissue/min
              for 4 to 6 rats.
                             20-

                             18-

                             16-

                             14-
                           5  8-

                           !  6H
                               2-
                                 0.02 mM Cd
         072345
                 mM Zn

Figure 2.     Effect of Zn on Cd uptake.


  (4) Step II in the absorption of Cd, i.e.,
     its movement from  mucosa into
     blood, proceeds  at only 1 -2%  of
     the rate of  Step I.  Step II is  in
     series with  Step I, and  under4
     present  conditions  determines^
     the rate of Cd absorption into the
     body.
  (5) Metallothionein, the low molecu-
     lar weight protein able to  bind 7
     moles Cd/mole, could  not be
     shown  to play  any role  in the
     aborption of Cd.
  (6) Cd  absorption in the duodenum
     resembles qualitatively that de-
     scribed  for the jejunum. In con-
     trast, Step II  of Cd transport is
      relatively much faster  in the
      ileum.
  This investigation has contributed to a
better def i nition of factors which  may be
responsible  for the  control  of Cd
absorption in vivo. In addition,  it has
confirmed the possibility  of altering
fractional absorption of an oral  load of
Cd by dietary manipulations.  Work
along these lines is continuing.
  The  results of this research have been
published intwojournalarticles: "Some
determinants  of intestinal cadmium
transport in the rat", by E.G. Foulkes, J.
Environ  Path  and Toxicol. 3.471-81
(1980), and  "On the role  of metallo-
thionem in cadmium absorption by  rat
jejunum in situ", by  D.  Kello  et al..
Toxicology 14:199-208 (1979).
                                                                                                                   I

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   £. C Foulkes, D R. Johnson, N Sugawara, R. F. Bonewitz, andC, Voner are with
      the University of Cincinnati, Cincinnati, OH 45267.
   Norman E. Kowal is the EPA Project Officer (see below).
   The complete report, entitled "Mechanisms of Cadmium Absorption in Rats,"
      (Order No.  PB 82-108 184: Cost. $8.00, subject to change) will be available
      only from
           National Technical Information Service
           5285 Port Royal Road
           Springfield, VA 22161
           Telephone  703-487-4650
   The EPA Project Officer can be contacted at
           Health Effects Research Laboratory
           U S  Environmental Protection Agency
           Cincinnati,  OH 45268
•ff U S GOVERNMENT PRINTING OFFICE 1982 — 559-017/7449

-------
   E. C. Foulkes, D. Ft. Johnson, N. Sugawara, R. F. Bonewitz, andC. Voner are with
      the University of Cincinnati, Cincinnati, OH 45267
   Norman E. Kowal is the EPA Project Officer (see below).
   The complete report, entitled "Mechanisms of Cadmium Absorption in Rats,"
      (Order No  PB 82-108 184. Cosf $8 00, subject to change) will be available
      only from:
           National Technical Information Service
           5285 Port Royal Road
           Spring field, VA 22161
           Telephone  703-487-4650
   The EPA Project Officer can  be contacted at
           Health Effects Research Laboratory
           U.S.  Environmental  Protection Agency
           Cincinnati,  OH 45268
•fa U S GOVERNMENT PRINTING OFFICE, 1982 — 559-017/7449

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