EPA/600/R-93/029
                                    February 1993
        ERL-DULUTH
    SPOTLIGHT ON
       RESEARCH
             1992
 Environmental Research Laboratory-Duluth
Office of Environmental Processes and Effects
   Office of Research and Development
  U.S. Environmental Protection Agency
                                Printed on Recycled Paper

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                   DIRECTOR'S PERSPECTIVE

     As we continue into the  90's,  our laboratory,  like the
rest of the  EPA,  is  in a period of change.   Our mission to
develop the  science needed  by EPA  in  creating environmental
policies for use of freshwater resources continues..  However,
there are  new areas of  emphasis  and  some past  research is
coming to a close. As  the vision for EPA and the role of ORD
evolves, we expect that additional changes will occur.

     ERL-Duluth and its Large Lakes Research Station in Grosse
lie, MI continue  to lead EPA's research effort on the Great
Lakes.   The  mass balance  modeling framework  for  lakewide
management  planning  was  successfully  demonstrated   in  the
multi-agency Green Bay  study.  Research to develop the science
necessary to improve and apply these models to whole lakes is
a major focus for the  laboratory.  Research on understanding
how  exotic   species   impact   freshwater  ecosystems  is  a
significant new area of study.  The  Ecological Monitoring and
Assessment Program (EMAP) research  conducted by ERL-Duluth is
providing   exciting   challenges  requiring   a  fundamental
understanding of how the -Great Lakes ecosystems  function.  In
all the Great Lakes research, research partnerships with other
agencies and academic institutions  provide  a solid foundation
for meeting these challenges.

     Our goal of developing the knowledge,  methods and models
to predict the toxicity of chemicals to aquatic life forms the
framework  for  much  of  the  laboratory's research.    The
laboratory  continues  to provide  a  substantial scientific
effort in understanding the effects of contaminated sediments
on freshwater life.  Within our predictive toxicology program,
reactive and bioaccumulatable chemicals are being emphasized.
Research  contributing  to  the  reassessment  of  the  risk of
dioxin to aquatic life  and wildlife is one of the laboratory^
highest priorities for thfe next few years.  We look upon this
as one of the most intensive integrative projects that we have
attempted.   At the same time, our effluent toxicity  program
completed  its  mission to  develop methods  for  identifying
chemicals  of  concern in  municipal and  industrial discharges.
Much  of  this knowledge has been successfully transferred to
the user community.

     Our ecology  program also continues  to change.  Research
to develop methods such!as littoral enclosures has evolved to
the development of models of  ecological  interactions  leading
to  predictions of ecological risk due to  chemical stresses.
Our  wetlands  research  is  directed   towards  understanding
relationships between  wetlands and water quality. Additional
research on Great Lakes coastal wetlands  is now: included as
part  of this mission.    Finally, we continue to develop new
approaches to protect  aquatic ecosystems through research on
watershed properties and non-point  sources  of stress that will
lead  to  improved  ecologically based criteria.

                              -i-

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                                    CONTENTS
                                                                                 'age

RESEARCH AREAS

Biotechnology	      1
Contaminated Sediments Research
      Quality criteria	      2
Databases
        ASTER	      3
        AQUIRE	      4
        QSAR	      5
Ecosystem Response	      5
Environmental Monitoring & Assessment Program (EMAP)	      7
Global Climate	      8
Introduced Species	      9
Nonpoint Source Characterization	     10
Point-Source Discharges/Effluent Characterization	     11
Risk Assessment
      Predictive toxicology	„	     12
      Wildlife criteria	     13
Sediment TIE Document	     14
Water Quality Criteria	     15
Watersheds	     16
Wetlands..	     17

RELATED ACTIVITIES

American Indian Program	     18
Environmental Education Outreach	     19
International Exchange	     20
Research Seminars	     21

Organizational Structure	     22
Recent Publications	     23
                                       -11 -

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                          Biotechnology
            One of our goals is to develop and evaluate laboratory test
    systems that portray how microorganisms may affect natural systems.
 These systems, called microcosms, are needed to evaluate new microbial pest
 control agents and new forms of microorganisms used in bioremediation
or by industry.

  We have developed and continue to test several types of microcosms.
TEMPOCORE is the name of one of the new systems. It is based on soil
 cores collected from a dried,, temporary pool of water. The cores contain
 resting or inactive stages of algae, zooplankton, protozoa and other fauna.
 When a core is placed in ajar and water is added, soon natural populations and
  natural nutrient concentrations will develop. After stabilizing, the populations
    provide all the functions, including predation, found in natural systems.
     Measuring effects of new microorganisms in such a system can
       produce an authentic measure of direct or indirect effects.
                       For more information contact
                      Dick Anderson (218) 720-5616


                                  -1-

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                 Contaminated Sediments Research -
                           Quality Criteria

        Guidelines for deriving Sediment Quality Criteria (SQC) are
   being examined to validate the ability of predictive EPT (Equilibrium
  Partitioning Theory) relationships to protect benthic communities.
 Tissue residue/toxicity relationships are being studied to establish cause
 and effect tissue concentrations to aid in the verification of SQC and the
development of food chain models.

     To perform reliable assessments of contaminated sediments for
regulatory/remediation activities it is necessary to have standard methods
such as bioaccumulation protocols and toxicity tests. ERL-D is
 developing test methods for contaminated sediments using three species:
 the amphipod, Hyalella azteca, the chironomid, Chironomus tentans,
  and the oligochaete, Lumbriculus variegatus. Some of the reasons for
   choosing these species include: a) ecological relevance, b) ability to
     assess acute and chronic toxicity endpoints, and c) ease of
      culturing and handling. ERL-D also is developing toxicity
         identification evaluation procedures for sediments to
           pinpoint contaminants responsible for toxicity in
             samples that theoretically, could contain             ,   "'
                 thousands of different chemicals.
                    For more information please contact
                      GaryAnkley  (218) 720-5603.
                                -2-

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                   DatabasesiASTER
         Assessment Tools for the Evaluation of Risk
     ' ASTER was developed by ERL-D to assist regulators in
  performing ecological risk assessments. ASTER is an integration of
 the AQUIRE (AQUatic toxicity Information REtrieval) toxic effects
 database and the QSAR (Quantitative Structure Activity Relationships)
system, a structure activity-based expert system. ASTER is designed to
provide high quality data for discrete chemicals when available in the
 associated databases and QS AR-based estimates when data are lacking.
 ASTER is currently available to governmental agencies through the
   U.S. EPA National Computing.Center. Training is available
    and consists of a brief overview and hands-on computer
               access to the ASTER system.
                For more information please contact
                Christine Russom (218) 720-5709.
                             -3-

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                       Databases: AQUIRE
             AOUatic toxicity Information REtrieval
       The AQUIRE database provides quick access to a comprehensive,
  systematic, computerized compilation of aquatic toxic effects data
 Scientific papers published both nationally and internationally on the
toxic effects of chemicals to aquatic organisms and plants are collected and
reviewed for AQUIRE. Independently compiled laboratory
data files that include AQUIRE parameters and meet the quality
assurance criteria are also included. Acute, sublethal and
bioconcentration effects are recorded for freshwater and marine
 organisms. AQUIRE consists of over 99,710 individual test results
  on computer file.  These tests contain information for 5,500 chemicals
   and 2,361 organisms, extracted from over 6,650 publications.  All
   AQUIIRE data entries have been subjected to established quality
    assurance procedures. AQUIRE is a VAX-bassed system located
       at the National Computer Center. The database can be accessed
        through the EPA network via the VAX system or through
                   a modem and personal computer.
                   For more information please contact'
                   Christine Russom (218) 720-5709.
                              -4 -

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                      Databases: QSAR
         Quantitative Structure Activity Relationship
\
       QS AR is an expert system which provides immediate information
   on physical-chemical properties, fate and effects of organic chemicals
  to the environment.  QSAR utilizes structure-activity relationships:
 statistical methods which relate the structure and physiochemical proper-
ties  'of compounds to biological activity. The QSAR system includes a
database of measured physiochemical properties such as melting point,
boiling point, vapor pressure, and water solubility as well as more than
 56,000 molecular structures stored as SMILES (Simplified Molecular
 Input Line Entry System) strings for specific chemicals. When
  empirical data are not available mechanistically-based predictive models
   are  used to estimate ecotoxicology endpoints, chemical properties,
   biodegradation, and environmental partitioning. QSAR is a VAX-
     based system located at the National Computer Center. The data
       base can be accessed through the EPA network via the VAX
         system or through a modem and personal computer.
                 For more information please contact
                 Christine Russom  (218) 720-5709.
                             -5-

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                      Ecosystem Response
                 We continue to develop and refine the
         littoral enclosure design and protocol for testing the effects
      of pesticides and other toxic compounds in natural aquatic ecosystems.
    Littoral enclosures are a mesocosm system designed to provide ecosystem
   effects information for use in the pesticide registration process.

      Littoral enclosures are also being used to provide statistically valid
ecosystem effects data to use to develop and test the Littoral Enclosure
Risk Assessment Model (LERAM).  The LERAM, developed from the
 Comprehensive Aquatic System Model (CASM), has predicted the effects
 observed in studies of littoral ecosystems exposed to different pesticide
  concentrations, and has provided risk assessments for each exposure level.
    In addition, LERAM provides information which can be used to design
      and evaluate field studies.
                       For more information please contact
                       Richard Siefert (218)  720-5552 or
                          Frank Stay (218) 720-5542

                                  -6-

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      Environmental Monitoring & Assessment Program
                          (EMAP)

         The EMAP-Great Lakes Program is an interagency,
     inter-disciplinary program whose goals are to estimate the current
  status, trends and changes in selected indicators of the condition of the
 Great Lakes with known confidence. Associations between selected
indicators of natural and anthropogenic stresses, and indicators of condition
are being examined. Statistical summaries and periodic assessments
 of the Great Lakes will be provided annuallly.  Each of the five lakes
  has been established as the regional scale of resolution and within
   each lake, four resource classes have been established for
      monitoring activities.
           For more information please contact
           Stephen Lozano,  (218) 720-5594.


                              -7-

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            Our long- term objective is to predict the nature,
      degree, and significance of global climate change effects on
    freshwater ecosystems. Initial research activities are focused on
   developing models for translating meteorological conditions associated
 with a doubling of CO2 levels in the atmosphere into changed water
quality conditions and fisheries resources. A procedure for estimating
regional effects of climate change on water temperature, thermal structure,
 dissolved oxygen, and fishes has been developed and reported in the
  literature.               !

      Future research will extend these impact analyses to other regions
        and integrate this model with those being developed to predict
           trophic dynamic responses and terrestrial effects.
                For more information please contact
                John Eaton  (218) 720-5557.
                              -8-

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                            Introduced Species
           The U.S. EPA research program on aquatic nuisance species is
      managed and conducted by research scientists at ERL-D. The objectives;
     are to develop an integrated, coordinated research program on aquatic
   nuisance species throughout the continental United States, focusing intitally
   on the Great Lakes and the Mississippi River basin. The program is in
 response to the Nonindigenous Aquatic Nuisance Prevention and Control Act of
1990, and is coordinated with other agencies through the Aquatic Nuisance
Species Task Force and it's committees.
       The approach has been to consider the problem of introduced species
from three aspects; as an interaction of (1) a species population with (2) a
vulnerable ecosystem to (3) produce effects. Under this framework ERL-D
is focusing intitally on several species which have demonstrated their ability
 to successfully invade lake and river ecosystems, including the zebra mussel,
 the ruffe (a fish) and the rusty crayfish. The role of natural disturbances in
  rivers and streams, caused by flow extremes, on vulnerability to invasion
   is being considered, as well as landscape factors in the surrounding
    watershed. Finally, projects are underway or planned on the
      accumulation and trophic transfer of organic chemicals by zebra
       mussels and their effect on nutrient and energy dynamics;
         metabolism and toxicokinetic of contaminants in zebra
           mussels; and the potential influence of zebra mussels
               on native benthic communities in the upper              '
                    Mississippi river and it's major tributaries.      /,'s
                       For more information please contact
                       J. David Yount  (218) 720-5752.
                                    -9-

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                 Nonpoint Source Characterization

              We have continued to determine the impact
        of agrichemicals on aquatic life.  This project is fulfilling certain
      objectives of EPA's Midwest Agrichemical Surface/Subsurface
    Transport and Effects Research  (MASTER) Plan that outlines research
   needs for the Walnut Creek Watershed located near Ames, Iowa and
  the western corn belt ecoregion.
     The U.S. Geological Survey and U.S. Department of Agriculture
Management Systems Evaluation Areas (MESA) Program has emphasized
research on the transport and fate of selected agrichemicals and effects on
water.  However, the ecotoxicological effects associated with varying
 farming systems and agrichemical loadings have not been addressed to
 date.  The goals of the research at ERL-D are to develop fate and
  ecotoxicological cause-and-effect information for typical classes of
    agriculture chemicals found in the surface waters of the midwest
     corn belt. This information will assist in developing
       diagnostic procedures and predictive techniques to describe their
          impacts on the well-being of aquatic life and to assess the
            environmental benefits of different ecosystem restorative
                techniques or alternate farm management systems.
                    For more information please contact
                    A. Ron Carlson (218) 720-5523.
                                  -10-

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                     Point-Source Discharges /
                     Effluent Characterization

            The complex effluent research program has had an active
      involvement in the development of the basic science and technological
    tools supporting the whole effluent toxicity based approach of EPA's
   water quality based effort to control toxics.

  Current effluent related research includes a) the development of toxicity
 identification evaluation (TIE) procedures for identifying the cause of  acute
 and chronic toxicity in effluents and ambient waters, b) the
 development of procedures for identifying, assessing, and controlling
 chemicals which cause chemical residues in fish and shellfish by
 bioconcentration and/or bioaccumulation processes, and c) the
  performance of field studies investigating the relationships between
   point source toxicity and ambient toxicity, and their impacts upon
              the biological structure in ambient (receiving) water.

      Guidance documents for performing TIE procedures for characterizing,
       identifying, and confirming the cause (s) of toxicity for acutely and
\        chronically  toxic freshwater effluents are available. The Phase I
  \.         document is available now. Phase n and in documents are
   '"*"-           being updated and will be published in March 1993.
                   For more information please contact
                   Lawrence Burkhard (218) 720-5554.
                                 -11-

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               Risk Assessment - Predictive Toxicology
          Efforts at ERL-D have been initiated to address a variety of new
    research and application issues associated with use of predictive
   toxicology models in ecological risk assessments. Research to support the
  use of quantitative structure activity relationships (QSARs), physiologically-
 based toxicokuietic models, and molecular dosimetry techniques in assessing
the hazards of chemical stresssors has been undertaken.

        Recent results have led to improved understanding of chemical
reactivity and studies involving xenobiotic metabolism and cellular
intoxication will provide the toxicologic knowledge base to develop
 second generation QS AR models for reactive toxicants. In turn,
  state-of-the-art analytical techniques are being perfected whereby the
  presence of potentially toxic reactive chemicals can be identified in
   sediments, leachates, or aquatic organisms.  These models help provide
      the means to relate environmental exposures to residue accumulation
          and adverse effects.
                 For more information please contact
                  Steven Bradbury (218) 720-5527.
                                -12-

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               Risk Assessment - Wildlife Criteria

        In response to an increasing need to assess the impact of chemical
    pollutants on wildlife that inhabit freshwater ecosystems, staff at the
  Environmental Research Laboratory-Duluth have been developing
 interim approaches to establish wildlife criteria.

       Mammalian- and avian- specific interim wildlife values for species
  associated with freshwater ecosystems were derived using a method
similar to that employed in the calculation of noncancer human health
criteria. Interim wildlife values for highly bioaccumulatable chemicals
 (e.g., 2,3,7,8-TCDD, DDT, mirex, PCB's, toxaphene, mercury and
 hexachlorobenze), are generally lower than both aquatic life arid human
  health ciriteria.  Wildlife and aquatic life values for inorganic metals
   are similar. This analysis is consistent with the wildlife criteria
    procedure described in the draft Great Lakes Water Quality Initative,
     which was developed in collaboration with EPA staff in the Office
       of Water as well as scientists in the Wisconsin Department of
          Natural Resources and the U.S. Fish And Wildlife Service.
                For more information please contact
                Steven Bradbury (218)  720-5527.
                               -13-

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                     Sediment TIE Document
        Contaminated sediments are of great concern because of their
    potential to affect water quality and exhibit in situ toxicity. The
   identification of specific sediment toxicants can provide a useful
  assessment tool for decisions on dredge disposal options, site remedial
  activities, as well as point source control efforts. Techniques for the
 identification of acute toxicants in complex effluents have been
 available for several years. Recent work at ERL-D has focused on
 adapting these toxicity identification evaluation (TIE) procedures to
contaminated sediments. Some of the modifications made for TIE work
with sediments were (1) determining an appropriate aqueous fraction for
 testing, (2) developing small-volume aqueous phase tests with
  benthic species, (3) developing alternative fractionation schemes
   for nonpolar organics not elutable in methanol, and (4) dealing
    with contaminants such as hydrogen sulfide not frequently found in
      effluents. A draft document detailing these modifications is
         available to interested parties.
                       For more information please contact
                         GaryAnkley (218) 720-5603.  'V
                                -14-

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                      Water Quality Criteria-Metals
             Current water quality criteria for metals were developed
         on the basis of total concentration of metal in laboratory test
      waters. The applicability of these criteria is uncertain because many
    natural waters have a higher fraction of total metals bound to suspended
   particles than laboratory test water. Metals on particles should be less
  bioavailable and the laboratory-derived criteria would therefore
 overestimate risk. One option to address these uncertainties is to use
dissolved metals as the basis for criteria. However, some studies have
suggested that paniculate metal might be partially bioavailable and could
therefore contribute significantly to toxicity when the dissolved fraction is
small.

        The acute toxicity of copper to fathead minnnows was studied in a
 series of tests in which different concentrations of suspended
 solids were added to test water, causing dissolved copper to range from
  20 to 80 percent. 96hr LCSO's ranged from about 100 to 350 ug/1 on the
   basis of total recoverable copper, but on the basis of dissolved copper
    the range was 60 to 90 ug/1, which is within the expected measurement
      of uncertainty. Tests of 30-day survival and growth of juvenile
       fathead minnows and acute mortality of Ceriodaphnia dubia also
         showed a better correlation to dissolved copper than to total
           copper, suggesting that dissolved copper does provide a
                better basis for assessing risk for these
          "'--„,       organisms and endpoints.               ,,;-•  '
                        For more information please contact
                        RussErickson (218) 720-5534.
                                   -15-

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                          Watersheds
              Diagnostic techniques are being developed to
        provide a framework for assessing watershed 'health' in terms
      of sediment and water quality, land use, habitat, and biological
   community structure. Cooperative projects are underway with the
  states of Minnesota and Michigan, and the U.S. Dept. of Agriculture in
 Iowa to test the diagnostic procedures in watersheds dominated by
agricultural activities. The gathered information is being consolidated
with discriminate statistical and geographic information system (GIS)
 methodologies to provide an interactive system to discern watershed
  stressors and the severity of degradation. Our results  so far indicate
  that the amounts of woody debris, stream-borne sediments and   '•
    elevated concentrations of ammonia and nitrates are important
      descriptors of basin quality. An additional use of this information
       is to provide state regulators a system for defining the watershed
           status and provide project goals useful for
              remediation activities.
\
                     For more information please contact '^
                       John Arthur (218) 720-5565.
                               -16-

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                               Wetlands

       The overall goal of the wetland research project is to provide the
   information needed to develop and evaluate management strategies for
  protecting the ecological integrity of wetlands. A number of studies in
 several types of wetlands are underway, or about to begin, on the effects of
 environmental stressors such as chemical pollutants and physical disturbances
on wetlands, and the functions wetlands perform in the landscape.

       Field mesocosms are used to determine the response of wetland
processes and biota to controlled ranges of chemical concentrations or
 conditions associated with a specific stressor.  Empirical field studies are used
 to compare "real world" wetland conditions and functions among small groups
  of wetlands along a gradient of environmental stressors. Studies to take
   place in the next five years include the responses of prairie pothole
    wetlands to excess sedimentation, the effects of management practices
       and nonpoint source pollution on bottomland hardwood forests, and
          the effects of storm water on urban wetlands.
                    For more information please contact
                    William Sanville (218) 720-5723.
                                 -17-

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                      American Indian Program
                 Over the past four years ERL-D's Human
            Resources Office, the Fond du Lac Indian Reservation, and
         the Center of American Indian and Minority Health have
       established a positive working relationship. As a result of this
     cooperative effort, several programs are in place and planned which
    benefit American Indian students.                                        \

       Our cooperative education program with the Ojibway School and the Duluth's
 Schools Dept. of Indian Education targets kindergarten through senior high school
students.  The objective of this program is to expose American Indian elementary
students to science, thereby increasing their interests. Internships for high school
students and K-12 teachers are available to foster interest in science, math, and bio-
medical careers. Students and teachers complete research projects over a four-
weekperiod each summer. ERL-D hosts a program for undergraduate science and-
bio-medical students. This program, through the Fond du Lac Reservation's Ni-Shou
 Gabawag grant, allows students to work with research teams for ten hours per week
  during the school year and full-time during breaks and summer vacations.

             We recently developed a pre-collegiate program with the Fond du
         Lac Community College. This community college is one of 27
           tribal colleges within the United States.  Through continued
               participation in these programs, ERL-D anticipates          ;
                    producing a small, steady stream of American
                           Indian  scientists in five years.
                       For more information please contact
                       Sherry Linder (218) 720-5543.


                                   -18-

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                  Environmental Education Outreach

             We continue to promote environmental education among area
        elementary students and teachers. The lab hosted area teachers at aquati^
      education workshops and we visited area schools using traveling displays to*
    give children "hands-on" experience in aquatic biology and chemistry. We
   were instrumental in the formation of a community-based EE advisory
  committee that will serve a seven county area. The group will prepare a resource
 guide which will include brief summaries of EE opportunities in this area and
distribute a regular newsletter.

             Staff members helped EPA's Region 5 to evaluate the technical
merits of grant proposals submitted under the EE Act of 1990 and volunteered to
serve as project officers for grants having emphasis on science activities. Other
volunteers participated in a program designed to encourage young women (150) to
 pursue careers in science. Our portion of the program focused on environmental
  sciences. Some of our scientists served as judges, mentors, or as committee
   members at science fairs.
            We also continue to sponsor in-house tours, especially for high
          school and college students, whenever scientists can spare time from
            their on-going research.
                     For more information please contact
                     Robert Drummond (218) 720-5733.
                                  -19-

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                     International Exchange

      In 1992 approximately 10 scientists from many countries of the
  world visited ERL-D. These men and women spent days or weeks
 interacting with ERL-D scientists. Some of the homelands represented
were Russia, Bulgaria, China, Brazil and Canada.

      ERL-D scientists traveled world-wide to share their expertise with
scientists in Findland, Sweden, Canada and Australia.

      We at ERL-D are proud to be part of the world-wide scientific
  community, and we expect this interaction to continue and to accelerate
   in the coming years.
                  For more information please contact "'
                    Evelyn Hunt (218) 720-5509.
                              -20-

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                        Research Seminars

         ERL-D scientists and staff members gather regularly to listen to
   seminars presented by their colleagues and other scientists from the
  United States, Canada, and other countries. Scientists share their
 accomplishments in their areas of interest and expertise.  Local and area
researchers from other institutions also attend these interesting and
illuminating lectures.

       In addition, scientists at ERL-D share their expertise by presenting
 poster sessions and giving formal papers at symposia such as the Society of
  Environmental Toxicology and Chemistry (SETAC) and the American
   Chemical Society.

                For more information please contact
                 Evelyn Hunt (218)  720-5509.
                            -21-

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                   RECENT PUBLICATIONS*


 Amato, J.R.,  D.I. Mount, E.J.  Durhan, M.T. Lukasewycz, G.T.
 Ankley,  and E. Robert.   1992.  An example of the identification
 of  diazinon as a primary toxicant in an effluent.  Environ.
 Toxicol.  and  Chem. 11:209-216.

 Ankley,  G.T.  and L.P. Burkhard.  1992.  Identification of
 surfactants as toxicants in a  primary effluent.  Environ.
 Toxicol.  Chem.  11:1235-1248.

 Ankley,  G.T., P.M. Cook, A.R.°  Carlson, D.J. Call, J.A. Swenson,
 H.F. Corcoran, and R.A.  Hoke.  1992.  Predicting the acute
 toxicity of copper in freshwater sediments:  Evaluation of the
 role of  acid  volatile sulfide.  Environ. Toxicol. Chem.  In
 Press.

 Ankley,  G.T., K. Lodge,  D.J. Call, M.D. Balcer, L.T. Brooke, P.M.
 Cook, R.G. Kreis, A.R. Carlson, R.D. Johnson, G.J. Niemi, R.A.
 Hoke, C.W. West, J.P. Giesy, P.O. Jones and Z.C. Fuying.  1992.
 Integrated assessment .of contaminated sediments in the Lower Fox
 River and Green Bay, Wisconsin.  Ecotoxicol. Env. Saf. 23:46-63.

 Ankley,  G.T., v.R. Mattson, C.W. West, and J.L. Bennett.  1992.
 Bioaccumulation pf PCBs  from sediments by oligochaetes and
 fisher:  Comparison of labortory and field studies.  Can. J.
 Fish. Aquat.  Sci.  In Press.

 Ankley,  G.T., M.K.. Schubauer-Berigan and R.A. Hoke.  1992.  Use
 of toxicity identification evaluation techniques to identify
 dredged  material disposal options:  A proposed approach.
 Environ. Manage.  16:1-6.

 Auer, M.T. and N.A. Auer.  1990.  Chemical stability of
 substrates for walleye egg development in the Lower Fox River,
 WI.  American Fisheries Soc.   119:871-876.  EPA-600/J-90/532.

 Broderius, S.J.   1992.  Modeling the joint toxicity of
 xenobiotics to aquatic organisms:  Basic concepts and approaches.
 In: Aquatic Toxicology and Risk Assessment:   Fourteenth Volume,
ASTM STP 1124.  M.A.  Mayes and M.G.  Barron,  Eds., American
 Society  for Testing and Materials, Philadelphia, pp.  107-127.

 Detenbeck, N.E.,  C.A. Johnston, and G.J.  Niemi.  1992.  Wetland
effects on lake water quality  in the Minneapolis/St.  Paul
metropolitan area.   Landscape.  Ecol.  In Press.
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 Doerger,  J.U.,  J.R.  Meier,  R.A.  Dobbs,  R.D.  Johnson,  and G.T.
 Ankley.   1992.   Toxicity reduction evaluation at a municipal
 wastewater treatment plant  using mutagenicity as an endpoint.
 Arch.'Environ.  Contam.  Toxicpl.  22:384-388.

 Durhan,  E.,  M.  Lukasewycz,  and S.  Baker.   1992.   Alternatives  to
 methanol/water SPE elution  for the fractionation of high log KOH
 organic  compounds in aqueous environment  samples.   J.
 Chromatography.  In Press.   ;                 .

 Eaton, J.G.,  W.A. Swenson,  T.D.  Simonson,  and K.M.  Jensen.   1992.
 A field  and laboratory  investigation of acid effects on large
 mouth bass,  rock bass,  black crappie,  and yellow perch.  American
 Fisheries Society.  In  Press.

 Glass, G.E.,  J.A. Sorensen,  K.W.  Schmidt,  J.K.  Huber,  G.R.  Rapp,
 Jr.,  M.E.  Brigham, and  P.L.  Brezonik.   1992.  • Mercury in the St.
 Louis River,  Mississippi River,  Crane Lake,  and Sand Point Lake:
 Cycling,  Distribution,  and  Sources.   Report  to  the Legislative
 Commission on Minnesota Resources.  Chapter  1.,  Executive
 Summaries, G.E. Glass,  J.A.  Sorensen,  K.W. Schmidt, J,,K. Huber,
 G.R.  Rapp, Jr., M.E. Brigham and P.L.  Brezonid;  Chapter 3.,
 Mercury  Sources and Distribution in Minnesota's Aquatic
 Resources:  Surface Water,  Sediments,  Plants, Plankton, Fish,
 Remediation,  and Methods, Glass,  G.E.,  J.A.  Sorensen,  K.W.
 Schmidt,  J.K.  Huber, G.R. Rapp,  Jr. ; Chapter 4.,  Mercury Sources
 and  Distribution in Minnesota's Aquatic Resources:   Deposition,
 Glass, G.E.,  J.A. Sorensen,  K.W.  Schmidt,  J.K.  Huber,  G.R.  Rapp,
 Jr.

 Heinis,  L.J.  and M.J. Knuth.  1992.   The  mixing,  distribution,
 and  persistence of esfenvalerate within littoral enclosures.
 Environ.  Toxicol. and Chem.  11:11-25.

 Herman,  L.J.   1992.   In expensive Environmental  Control Chamber
 for  Holding Fish.  Prog.  Fish-Cult.   54:132.

 Hermanutz, R.O.  1992.   Malformation of the  fathead minnow
 (Pimephales promelas) in an ecosystem with elevated selenium
 concentrations.  Bulletin of Environ.  Contam. and Toxicol.
 49:290-294.

 Hermanutz, R.O. K.N. Allen,  T.  H.  Roush,  and S.F.  Hedtke.   1992,,
 Effects  of elevated selenium concentrations  on  bluegills (Lepomis
 inacrochirus)  in outdoor experimental streams.  Environ. Toxicol,,
 and  Chem.   11:217-224.

 Hoffman,  A.D.,  S.L.  Bertelsen,  and M.L. Gargas.   1992,,  An in
 vitro gas equilibration method for determination of chemical
 partition coefficients  in fish.   Comp.  Biochem.  Physiol. 101A:47-
• 51.
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Hoke, R.A., J.P. Giesy, and R.G. Kreis, Jr.  1992.  Sediment pore
water toxicity identification in the Lower Fox River and Green

Bay, WI, using the Microtox. assay.  Ecotox. Environ. Saf.
23:343-354.

Johnson, R.D.  1992.  Absence of liver tumors in bullheads
collected from the Lower Fox River and Green Bay, WI.  J. Great
Lakes Research.  In Press.

Knuth, M.L.  1992.  The accuracy and precision of pesticide
concentrations following application to littoral enclosures.
Proceedings of the 18th Annual Aquatic Toxicity Workshop.  A.J.
Niemi and M.C. Taylor, editors.  September 30-October 3, 1991,
Ottawa, Ontario, Canada.

Knuth, M.L. and L.J. Heinis.  1992.  Dissipation and persistence
of chlorphyrifos within littoral enclosures.  J. Ag. Food Chem.
40:1257-1263.

Leino, R.L., and J.H. McCormick.  1992.  Response of juvenile
largemouth bass to different pH and aluminum levels at
overwintering temperatures:  Effects on gill morphology, scale
calcium, liver glycogen, depot fat, and electrolyte balance.
Can. J. Zool.  In Press.
                                           0
Leino, R.L., J.H. McCormick, and K.M. Jensen.  1992.  Long-term
effects of an acute acid pulse on juvenile black crappie, Pomoxis
nigromaculatus.  Proceedings of the 18th Annual Aquatic Toxicity
Workshop: September 30-October 3, 1991.  Ottawa, Ontario, Canada.

Lukasewycz, M. and E.J. Durhan.  1992.   Strategies for the
identification of non-polar toxicants in aqueous environmental
samples using toxicity-based fractionation and gas
chromatography/mass spectrometry.  J. Chromatog: Biomedical
Applications.  580:215-228.

Marchini, S., M.L. Tosato, T.J. Norberg-King, D.E. Hammermeister,
and M.D. Hoglund.  1992.  Lethal and sublethal toxicity of
benzene derivatives to the fathead minnow, using a short term
test.  Environ. Toxicol. Chem.  11:187-195.

McCormick,  J.H. and K.M. Jensen.  1992.  Osmoregulatory failure
and death of first-year largemouth bass (Micropterus salmoides)
exposed to low pH and elevated aluminum,  at low temperature in
soft water.  Can. J.  Fish. Aq.  Sci. 49:1189-1197.
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McKim, J.M. and J.W. Nichols.   1992.  Use of Physiologically-
based toxicokinetic models  in a mechanistic approach, to  aquatic
toxicology.  Book Chapter.  In  Press.

Phipps, G.L.., G.T. Ankley,  D.A. Benoit, and V.R. Mattson.   1992.
Use of the aquatic oligochaete  Lumbriculus variegatus  for
assessing the toxicity and  bioaccumulation of sediment-associated
contaminants.  Environ. Toxicol. Chem.  In Press.

Rossmann, R.  1992.  Historical Trends of Chlorides  in the  Great
Lakes.  In - Deicing Chemicals  in the Environment, R.M.  D'ltri
(Ed.), Lewis Publishers, Chelsea, Michigan.  pp. 303-322.

Schmieder, P.K. and L.J. Weber.  1992.  Blood and water  flow
limitations on gill uptake  of organic chemicals in the rainbow
trout (Onchorynchus mykiss) .  Aq. Toxicol. 24:103-122,,

Schubauer-Berigan, M.K., J.R. Amato, G.T. Ankley, S.E,, Baker,
L.P. Burkhard, J.R. Dierkes, J.J. Jenson, M.T. Lukasewycz,  and
T.J. Norberg-King.  1992.   The  behavior and identification  of
toxic metals in complex mixtures: examples from effluent and
sediment pore water toxicity identification evaluations.  Arch.
Environ. Contam. Toxicol.   In Press.

Sierszen, M.E. and T.M. Frost.  1992.  Selectivity in  suspension
feeders:  Food quality and  the  cost of being selective.  Arch.
Hydrobiol.  123:257-273.

Smith, V.E., J.E. Rathburn, and J.C. Filkins.  1992.   Sampling,
characterizing and mapping  contaminated sediments in river
harbors.  Haz. Mat. Contr.  In  Press.

Spefan,  H.G., J.G. Eaton, M.: Hondzo,- B,E= Hoodno, X, Fang,  K.E.F.
Hokanson, and J.H. McCormick.   1992.  A methodology to estimate
global climate change impacts on lake water and fisheries in
Minnesota.  Proceedings, First  National Conference on  Global
Climate Change and Water Resources Management.  In Press.

Stay, F.S. and A.W. Jarvinen.   1992.  Selection of treatment
concentrations for field studies using data from MFC microcosms
and fish single species toxicity tests.  ERL-Duluth Internal
Report.   Deliverable #5657.  74pp.  EPA 600/X-92-104.

Tillitt, D.E., G.T. Ankley, J.P. Giesy, J.P. Ludwig, H.K.
Matsuba, D.V. Weseloh, P.S. Ross, C.A. Bishop, L. Sileo, K.L.
Stromborg, J. Larson, and T.J.  Kubiak.  1992.  Pdlychlorinated
biphenyl residues and egg mortality in double-crested  cormorants
from the Great Lakes.  Environ. Toxicol. Chem.  11:1281-1288.
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    * Many of our products are available in the open  literature
and in books.  EPA  reports may be obtained by writing to:

     Center for Environmental Research Information  (CERI)
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or purchased from the

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     Also available  are:

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          EPA-600/3-90/071.
                               -27-
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