United States Air and Energy Engineering
Environmental Protection Research Laboratory
Agency Research Triangle Park NC 27711
Research and Development EPA/600/S8-90/053 Sep. 1990
&EPA Project Summary
Recommended Operating
Procedure No. 45: Analysis of
Nitrous Oxide from Combustion
Sources
Judith S. Ford
This recommended operating pro-
cedure (ROP) has been prepared for
use in research activities conducted
by EPA's Air and Energy Engineering
Research Laboratory (AEERL). The
procedure applies to the measure-
ment of nitrous oxide (N2O) in dry
gas samples extracted from gas
streams where N2O concentrations
range from 0.5 to 200 parts per million
(ppm). N2O concentrations are inter-
preted by an electron capture detec-
tor (ECD). The ECD uses a 63Ni
constant current cell. The upper
limits of this procedure can be exten-
ded by changing the sample loop
pressure to reduce the volume of
sample in the loop or by diluting the
sample.
ROPs describe non-routine or
experimental research operations
where some judgment in application
may be warranted. ROPs may not be
applicable to activities conducted by
other reserach groups and should
not be used in place of standard
operating procedures. Use of ROPs
must be accompanied by an under-
standing of their purpose and scope.
This Project Summary was
developed by EPA's Air and Energy
Engineering Research Laboratory,
Research Triangle Park, NC, to
announce key findings of the research
project that is fully documented in a
separate report of the same title (see
Project Report ordering information at
back).
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Judith S. Ford is the EPA Project Officer (see below).
The complete report, entitled "Recommended Operating Procedure No. 45:
Analysis of Nitrous Oxide from Combustion Sources," (Order No. PB 90-
238 502/AS; Cost: $15.00, subject to change) will be available only from:
National Technical Information Service
5285 Port Royal Road
Springfield, VA 22161
Telephone: 703-487-4650
The EPA Project Officer can be contacted at:
Air and Energy Engineering Research Laboratory
U.S. Environmental Protection Agency
Research Triangle Park, NC 27711
United States Center for Environmental Research
Environmental Protection Information
Agency Cincinnati OH 45268
Official Business
Penalty for Private Use $300
EPA/600/S8-90/053
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