vvEPA
                         United States
                         Environmental Protection
                         Agency
                                   Risk Reduction
                                   Engineering Laboratory
                                   Cincinnati, OH 45268
                         Research and Development
                                    EPA/600/S-94/008  September 1994
ENVIRONMENTAL
RESEARCH   BRIEF
                  Waste Minimization Assessment for Manufacturer
               of Gravure-Coated Metalized Paper and Metalized Film

                             Richard J. Jendrucko*, Thomas N. Coleman*,
                                      and Gwen P. Looby**
Abstract
The U.S. Environmental Protection Agency (EPA) has funded
a pilot project to assist small and medium-size manufacturers
who want to minimize their generation of waste but who lack
the expertise to do so. In an effort to assist these manufactur-
ers Waste Minimization  Assessment Centers  (WMACs) were
established at selected universities, and procedures were
adapted from the EPA  Waste Minimization Opportunity As-
sessment Manual (EPA/625/7-88/003, July 1988). That docu-
ment has been superseded by the Facility Pollution Prevention
Guide (EPA/600/R-92/088, May 1992). The WMAC team at the
University of Tennessee performed an assessment at a plant
that manufactures gravure-coated metalized paper and film.
White coated paper purchased as a raw material is coated with
a water-based or solvent-based mixture, and a thin layer of
aluminum is deposited on the coating. Another coating is ap-
plied on top of the metalized surface. Rolls of film bought by
the plant also receive a thin layer of aluminum. The team's
report, detailing findings and recommendations, indicated that
a large quantity of solvent evaporates from the plant's pro-
cesses and that a large quantity of unused coating mixture is
wasted.  The greatest cost savings can  be achieved by the
plant through the installation of an automated  system for mix-
ing and diluting coating mixtures.

This Research Brief was developed by the principal investiga-
tors and EPA's Risk Reduction Engineering Laboratory, Cincin-
nati, OH, to announce key findings  of an ongoing research
project that is fully documented in a separate report of the
same title available from University City Science Center.
* University of Tennessee, Department of Engineering Science and Mechanics.
** University City Science Center, Philadelphia, PA.
                        Introduction
                        The amount of waste generated by industrial plants has be-
                        come an increasingly costly problem for manufacturers and an
                        additional stress on the  environment. One solution to the
                        problem of waste generation is to reduce or eliminate the
                        waste at its source.

                        University City Science Center (Philadelphia, PA) has begun a
                        pilot project to assist small and medium-size manufacturers
                        who want to minimize their generation of waste but who lack
                        the in-house expertise to do so. Under agreement with EPA's
                        Risk Reduction Engineering Laboratory, the Science Center
                        has established three WMACs. This assessment was done by
                        engineering faculty  and students  at the University  of
                        Tennessee's WMAC. The assessment teams have consider-
                        able direct experience with process operations in manufactur-
                        ing plants and also have the knowledge and skills needed to
                        minimize waste generation.

                        The waste minimization assessments are done for small and
                        medium-size manufacturers at no  out-of-pocket cost to the
                        client. To qualify for the  assessment, each client must fall
                        within Standard Industrial Classification Code 20-39, have gross
                        annual sales not exceeding $75 million, employ no more than
                        500 persons, and lack in-house expertise in waste minimiza-
                        tion.

                        The potential benefits of the pilot project include minimization
                        of the amount of waste generated by manufacturers and re-
                        duction of waste treatment and disposal costs for participating
                        plants. In addition, the project provides valuable experience for
                        graduate and undergraduate students who participate in the
                        program and a cleaner environment without more regulations
                        and higher costs for manufacturers.

                                                
-------
Methodology of Assessments
The waste minimization assessments require several site visits
to each client served. In general, the WMACs follow the proce-
dures  outlined  in the EPA Waste Minimization Opportunity
Assessment Manual (EPA/625/7-88/003, July 1988). The WMAC
staff locate the sources of waste in the plant and identify the
current disposal or treatment  methods and their associated
costs.  They then identify and analyze a variety of ways  to
reduce or eliminate the waste. Specific measures to  achieve
that goal are recommended and the essential supporting tech-
nological and economic  information is developed. Finally, a
confidential report that details the WMAC's findings and recom-
mendations (including cost savings, implementation costs, and
payback times) is prepared for each client.              '


Plant Background
The plant produces gravure-coated metalized paper and metal-
ized polypropylene  and polyester film for use in  labeling and
wrapping food products. It operates 8,760 hr/yr to produce >  14
x 10* Ib/yr of product.
                                                     [

Manufacturing Process
The plant's products are manufactured from raw paper and film
received in bulk rolls. Other raw materials include water-based
and solvent-based coating mixtures, aluminum wire (for vapor
deposition coating), liquid nitrogen,  and diluting solvents.  ;

Diluting solvents (three different organic-solvent-based coating
mixtures and a water-based coating mixture)  are receiveqi in
bulk quantities  and stored. The organic-solvent-based coating
mixtures are diluted with methyl ethyl ketone (MEK) as:re-
quired and transported to the pre-coater. Water-based coating
mixture is diluted with isopropanol and transported to eitherithe
pre-coater or top-coater.

Raw white coated paper  is processed in the pre-coater where
a coating is  applied to enhance the gloss of the paper knd
provide a good surface  for aluminum adhesion during l^ter
vacuum metalization. Two  coatings are applied to the paper,
and in some cases, both  sides of the paper are coated. On£ of
the three organic-solvent-based coatings or the water-based
coating is used  for each  coating  application;  the first jand
second coating applications may or may not use the same
coating mixture. Following coating, the paper is dried in: the
pre-coater oven.                                      ;

Each  coated paper roll from the pre-coater is transported to
one of two vacuum  metalizers. Rolls of polypropylene and
polyester film are processed in a specialized vacuum metalizer.
A thin layer of aluminum is deposited on the paper  and .film
through vapor-deposition. About half of the metalized film is  cut
to  specification in the metalizer and sent directly to shipping.
The rest of the film is sent to the finishing, rewind, and slitting
area of the plant prior to  shipping.                      :

The metalized  paper is transported to the top-coater  where a
coating is applied to the metalized surface in the same mariner
that the initial coating was applied  in the pre-coater. The top
coat (supplied  by the water-based coating) acts as a printing
primer and provides a clear protective layer. The coated paper
Is dried In the top-coater  oven and sent to the finishing, rewind,
and slitting area prior to shipping.

An abbreviated process flow diagram is shown in Figure 1i
      MEK
   isopropanol

 Water-based and
   solvent-based
 coating mixtures
    White coated
      paper


   Polypropylene
   film, polyester
    film, Al wire,
     liquid N2
                            Metalized
                          1 paper and film
Figure 1.  Abbreviated process flow diagram.


Existing Waste Management Practices
This plant operates an onsite solvent recovery still to recover
MEK from solvent wastes. Recovered solvent is used for dilut-
ing coating mixtures and cleanup.


Waste Minimization Opportunities
The type of waste currently generated by the plant, the source
of the waste, the quantity of the waste, the waste management
method,  and the annual waste  management cost for  each
waste stream identified are given in Table 1.

Table 2 shows the opportunities for waste minimization that the
WMAC team recommended for  the  plant. The minimization
opportunity, type of waste, the possible  waste reduction and
associated savings, and the implementation cost along with the
simple payback time  are given in the table. The quantities of
waste currently generated by the  plant and  possible waste
reduction depend on the production  level  of the plant. All
values should be considered in that context.

It should be noted that the financial savings of the minimization
opportunities result from the  need for less  raw material and
from reduced present and future costs associated with waste
management. Other savings not quantifiable by  this study in-
clude a wide variety of possible future costs related to chang-
ing emissions standards, liability, and employee health. It also
should be noted that the savings given for each  opportunity
reflect the savings achievable when implementing each waste
minimization opportunity independently and do not reflect du-
plication  of savings that would  result when the opportunities
are implemented in a package.

This research brief summarizes part of the work done under
Cooperative Agreement  No. CR-814903 by the University City
Science Center under the sponsorship of the U.S. Environmen-
tal  Protection  Agency.  The  EPA Project Officer was Emma
Lou George.

-------
-I
 §
CD
I
•ffi £
^ a
• — . c-
it
•*§
i





Waste Management
Method
ft
^5 q3
i|
^:u









Source of Waste









Waste Generated

o o o o
CM '•o CM co
3; CO^ K K
O) CO







Shipped offsite
Evaporates to plant air
Shipped offsite
Shipped offsite
o o o o
"St- *O 00 U>
C\J






O)
••£=
0
CD
fe
Solvent storage
Mixing and supply drums in j
Coating-mixture storage
Mixing of coating mixture

a £
CB 2
•5 5
i g>
§tn -i=
..
m "^3
CO *- »-C CD
•se .0 3 to
03 •?= t! CB
Isopropanol spills and le
Organic solvent evapora
Water-based coating mh
Off-specification water-b

1 1
§


^
CD
x_-
fi
5
Baled; sold to recycler
Ducted to onsite incine*
1 1
O) fS,











Pre-coating
Drying during pre-coating







^
.8
Waste paper
Organic solvent evapora

1 °



c
CD
j^.
^
£?
Ducted to onsite incinei
Evaporates to plant air
1 1
§j §>











Drying during pre-coating
Drying during top-coating









Isopropanol evaporation
Isopropanol evaporation

1 'I
t- irf







Evaporates to plant air
Shipped offsite
CO CO
CD" IO-



CS
c:
•s
0
V ir
& TO
1 ?
ci 9-
Supply drums in pre-coating
Cleaning ofpre-coater and tc




£
a
S
C3>
-g
Isopropanol evaporation
Unused water-based coa

^ 2
CO M-
CM" S~





^
•fc«
Shipped offsite; incinen
Shipped offsite
c^ c*\
oo co
CO V
^ !>"







n* n"
TO TO
? V
& B.
Cleaning ofpre-coater and tc
Cleaning ofpre-coater and tc





'c*
. ^
8> §

Solvent-soaked cleaning
Spent isopropanol cleanh

o o
S S
M-







Sold to recycler
Vented from plant
8 8
§" S
§










Vacuum metalizer
Vacuum metalizer









Scrap aluminum
Nitrogen gas

*— "SI-
CM co
1







Shipped to landfill
Shipped to landfill
O Oo
10 §>"











Vacuum metalizer
Vacuum metalizer




1
8
^
^
•S3
Polypropylene and poly et
Cardboard cores

§ §
co" cvT







Evaporates to plant air
Shipped offsite
8 S
10" co"







v^ v»
CtJ CB
0 0
V V
4 Q
Cleaning ofpre-coater and to,
Cleaning ofpre-coater and to,








M
Organic solvent evaporat
Spent organic solvent

i
*-*







Reused onsite
s
CM








§
••5
CO
*fc
Spills and leaks and off-sped
and unused coating mixture









Recoverable solvent

p> c\
c? '*







Shipped offsite
Shipped offsite
S §
CO *~"











Onsite distillation unit
Onsite distillation unit









Still bottoms
Dry coating residue













?
.s
01
3
C

15 |
O CO
-2J8
'i »
S R
g costs and applicable raw m&
dling waste plus raw material <
S c
cf
-c 2
? 9
•— - n
o 5
•f"^-

c" e
* Includes waste treatme
' Net cost of waste streai

-------

.1
.C
1
\
o-

"5
I
I
03^
H- £>
S5f

c
.0

§ ^°
"B.
^
'<3
is*
11
.1 1
S
1
i
1 t
1 !
o




^
Waste Stream Reduc




\
c

CO
•^



o
§-
s

§
s
£
§i^§§



IO CO "*}• CO IQ tO
CM

£
E
S> 95
••§3
i'l
Off-specification water-based
Unused water-based coating i
Still bottoms
Dry coating residue
Organic solvent evaporation
Isopropanol evaporation




Install a system to automate the
mixing and diluting of coating
mixtures to reduce unnecessary
waste and solvent evaporation.
%
'•Q
1



O




s"

\



l






Solvent-soaked cleaning rags




Contract with an outside firm to
clean rags and return them to
the plant for reuse.

Y-
^



o
CM


g
CO
10"

S8



o o






Organic solvent evaporation
Isopropanol evaporation




Cover drums containing coating
mixture during pre-coat and top-
coat operations to reduce
evaporative losses.
TO
•3
Qi

.g


0



1

-------

-------

-------

-------
United States
Environmental Protection Agency
Center for Environmental Research Information
Cincinnati, OH 45268

Official Business
Penalty for Private Use
$300
     BULK RATE
POSTAGE & FEES PAID
        EPA
   PERMIT No. G-35
EPA/600/S-94/008

-------