United States
                    Environmental Protection
                    Agency	
Risk Reduction
Engineering Laboratory
Cincinnati, OH 45268
                    Research and Development
EPA/600/SR-92/048   April  1992
& EPA      Project Summary
                     Removing  Radium  from Water  by
                     Plain  and Treated Activated
                    Alumina
                    Deepak Garg and Dennis Clifford
                      This research determined the feasi-
                    bility of using BaSO4-impregnated acti-
                    vated alumina and plain activated alu-
                    mina for radium removal from ground-
                    water by fixed-bed adsorption. The ma-
                    jor factors influencing radium adsorp-
                    tion onto the two types of alumina were
                    identified. The radium regemerability of
                    the aluminas was also studied.
                      Good to excellent radium  removals
                    were obtained depending on the chemi-
                    cal composition of the feedwater. For
                    example, BaSO4-impregnated alumina
                    treated 25,000 bed volumes  (BV) and
                    plain alumina treated 14,000  BV of in-
                    fluent before radium maximum contami-
                    nant level (MCL) breakthrough.
                      The presence of sulfate ions in the
                    feedwater enhanced  and the  presence
                    of barium inhibited radium adsorption
                    on both types of alumina. The water
                    hardness significantly reduced radium
                    removal by plain alumina although it
                    had little effect on radium removal by
                    BaSO4-impregnated alumina.  The
                    amount of BaSO4 contained in the im-
                    pregnated alumina correlated  positively
                    with radium adsorption.
                      When acid/base regeneration was em-
                    ployed,  BaSO4-impregnated  alumina
                    was  about 45%  regenerable with re-
                    spect to radium and  plain alumina was
                    about 70% to 95% regenerable. Excel-
                    lent performance was obtained when
                    using BaSO -impregnated alumina to
                    treat  actual  radium-contaminated
                    groundwater in Lemont, IL, where
                    25,000 BV could be treated before the
                    5 pCi/L MCL was reached. The best per-
                    formance with plain alumina was 12,000
BV when treating a Houston ground-
water spiked with 23 pCi/L of radium.
  This Project Summary was developed
by EPA's Risk Reduction Engineering
Laboratory, Cincinnati, OH, to announce
key findings of the research project
that is fully documented in a separate
report of the  same title (see Project
Report ordering information at back).

Introduction
  The ability of BaSO4 precipitates to re-
move radium from solution has been
known for more than 40 yr. Copreciprtation
of RaSO4 with BaSO4 is the standard tech-
nique used to concentrate radium in analy-
sis procedures for radium isotopes. The
Dow Radium Selective Complexer (RSC)'
is an experimental adsorbent that makes
good use of the  knowledge that BaSO4
scavenges radium from solution. With the
RSC, BaSO4 is impregnated into cation-
exchange beads. The work reported here
began with a similar idea, i.e.,  if BaSO4
could be effectively precipitated within the
pores of activated alumina, the resultant
material would serve as a good, inorganic,
radium-selective adsorbent. Activated alu-
mina is known to have a good capacity for
sulfate and, thus, was expected to be a
good host for sulfate before the precipita-
tion of BaSO . Plain activated alumina was
hot expected to be a good adsorbent for
radium but was tested for radium capacity
in control experiments. In fact, a survey of
the literature indicates that this is prob-
ably the first study done on the adsorption
of radium onto alumina of any kind.
  Mention of trade names or commercial products does
  not constitute endorsement or recommendation for
                                                                    Printed on Recycled Paper

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  BaSO4-impregnated alumina was pre-
pared in several ways, both in this study
and in field studies. The resultant alumina
was used to remove radium by fixed-bed
adsorption. Initial results indicated that not
only did this  material remove radium from
spiked Houston tap  water from a surface
source, but that plain activated alumina,
used for the control experiment, also gave
good results. Further experimentation with
BaSO,-impregnated alumina, plain alu-
mina, ana different types  of  feedwaters
resulted  in widely variable behavior in
terms of  radium removal. Very good ra-
dium removal was obtained with natural
waters, whereas essentially  no removal
was  obtained  with  synthetic  waters. At
this stage, we concluded that some con-
stituent of the natural waters, not present
in the  synthetic waters,  was responsible
for the removal of radium and thus, initi-
ated a study of the influence of pH, chlo-
ride, sutfate, and  total  organic carbon
(TOO). A general objective of the lab stud-
ies with  various waters was  to explain
how radium  is removed from natural wa-
ters by BaSO4-impregnated alumina and
plain alumina.
  The  effect of naturally occurring  organ-
tea, measured as TOG, on radium adsorp-
tion was  thoroughly investigated. We  ex-
pected that some preferential association
of the  Raa*  ions with the  predominantly
negatively charged natural organics would
exist  Organics were  found to  enhance
radium removal, but not enough  to  ex-
plain the  previously observed radium re-
moval, with natural waters. When we again
searched the literature to resolve the con-
fusion  generated by the  experimental re-
sults, we  found that  RaSO. ion pairs tend
to form in water when sultate is present
and that these uncharged species tend to
be adsorbed on all  surfaces,  particularly
glass.
  Finally, in  an effort to  establish  the
regenerabil'rty of the aluminas, acid/base
regenerations were attempted  on radium-
saturated samples of plain and of BaSO4-
Impregnated alumina.
  When the  experiments were finished, a
statistical analysis of the  data established
the effect of independent variables such
as pH, feed  ^Ra activity,  and the  back-
ground concentration  of sulfate, barium,
hardness, and TOO on the adsorption of
radium onto both BaSO4-impregnated and
plain alumina.
  Thus, the major objectives of this study
were:
  1.   to  determine  the  effectiveness of
      BaSO.,-impregnated  alumina  in re-
      moving radium from water by fixed-
      bed adsorption,
  2.  to determine the  effectiveness of
      plain activated alumina in removing
      radium from water by fixed-bed ad-
      sorption, and to compare its radium
      removal performance with that ob-
      tained with BaSO4-impregnated alu-
      mina,  '
  3.  to identify the water quality factors
      influencing  radium adsorption onto
      both BaSO4-impregnated and onto
      plain alumina,
  4.  to evaluate the regenerability of both
      BaSO4-impregnated and plain alu-
      mina, using acid and base, and fi-
      nally
  5.  to develop a set of rules for choos-
      ing the proper alumina — BaSO4-
      impregriated or  plain — to be ap-
      plied to water to remove radium.

Materials and  Methods

Preparation of Barium-Sulfate-
Impregnated Alumina
  Alcoa F-1 activated alumina (28 x 48
mesh, i.e., 0.$ x  0.3 mm diameter) was
used throughout the study. To utilize the
well-known radium  removal capacity of
BaSO4 as wel) as the  large surface area
present  within 'the alumina, we attempted
to impregnate BaSO4 into the alumina. To
achieve impregnation, sulfate was  first
adsorbed  onto the alumina then BaSO4
was precipitated within the alumina pores
by adding excess barium in the form of
BaCI2.
  The following reaction sequence  is pro-
posed for impregnating barium sulfate into
the alumina pores:
  Sulfation of the  activated alumina
=AI-OH + H,S04
                     =AI-HSO
                                  (1)
             ;
  Precipitation! of BaSO4 in activated alu-
mina
2=AI-HS04 + Bad, - > 2 =AI-CI +
  BaS04(s) + !H2S04                (2)

  Before being studied in detail in these
laboratory studies, BaSO -impregnated
alumina was  prepared and used  in the
U.S. Environmental Protection  Agency-
(EPA) funded, Lemont, IL, radium-removal
field study (Clifford et al., J. AWWA, 90:94-
104; July 1988). The  BaSO4-loaded alu-
mina was prepared in  a  1 -in.-diameter
glass column by slowly rinsing a 30-in.
deep bed of plain alumina with 10 BV of
0.25 N H2SO4 followed  by 10 BV of 0.25 N
BaCL The column was extensively rinsed
(40 BV) with reverse osmosis (RO) prod-
uct water to eliminate BaSO4(s) fines. Ra-
dium  adsorption tests with the BaSO4-
loaded alumina were  carried  out  in the
column  used to  prepare the medium.  A
control run with plain alumina was carried
out in Lemont in a similar 1-in.-diameter
column with a 20-in. depth of medium. A
similar impregnation procedure was used
for the laboratory experiments except that
0.5 N H28O4 and 1.0 N BaCI2 were used.
Normally, impregnations were carried out
at 22' to 25°C and 1  atm pressure. Higher
temperature (70°C), vacuum (25 mm  Hg),
and higher pressure (2 atm) techniques
were, however, briefly experimented with.

Minicolumn Experiments
  To reduce the volume of radium-spiked
water needed and to increase the number
of column runs that could be completed,
we used minicolumns of alumina contain-
ing approximately 5 cm3 of  medium. Nu-
merous previous experiments over a pe-
riod of six  yr  had shown that such  col-
umns could reliably be substituted for the
larger (1-in.-diameter) columns normally
used For adsorption  experiments.  The
minicolumns used in this research were
made of clear acrylic plastic, 10-in. (25.4
cm) long with an  i.d. of 0.25 in. (6 mm).
  The experimental  minicolumn flow  sys-
tem consisted of a feed solution contained
in a 13-gal (50  L)  polyethylene  carboy
pumped first through a 5-(im, in-line mem-
brane filter (with porous prefilter) and then
through the  minicolumn. Although pump-
ing pressures less than 20 psig (138 kPa)
were  required, a Milton Roy Laboratory
Data Control (model 396), high-pressure
metering pump was used  as  the  feed
pump. Generally the flow rate through the
5 cm3 of granular 28 x 48 mesh alumina
was maintained at 1.5 mL/min for an empty
bed contact time  (EBCT) of 3.3 min.
  The radium adsorption performance of
a column run was determined by analyz-
ing the feed and effluent for radium.
  The ^Ra isotope standard used in these
experiments for spiking the feedwater, was
calibrated and supplied by the EPA's En-
vironmental  Monitoring Systems Labora-
tory in Las Vegas, NV.
  One focus of this study was to examine
the effect of the presence of natural or-
ganics in feedwater  on the removal of
radium on  alumina. The  organics were
isolated from Lake Houston water with the
use of RO concentration, followed by  size
fractionation using uttrafiltration. The frac-
tions had cut-off limits of 10,000 (10K),
5,000 (5 K),  and 1,000 (1  K), apparent
molecular weight units (AMU). The 1  to 5
K and the 5 to 10 K fractions were  used
for the TOC spiking experiments because
these relatively smaller molecules were
expected to be at least partially adsorbed
by the aluminas.

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Batch (Isotherm) Experiments
  Activated alumina used in the batch iso-
therm experiments was ground and sieved
to less than 250 u.m in diameter (100%
passed through a U.S. Standard Sieve
No. 60) to facilitate the  kinetics of the
adsorption process. The alumina was then
transferred to five different bottles for pH
adjustment with 1 N NaOH or 1  N HCI.
This was done over a period of  2 days
with continuous shaking and monitoring of
pH. The water was decanted and the alu-
mina dried in an oven overnight. The alu-
mina was then exposed to  the atmosphere
for 6 hr to  ensure that  its weight  was
stable. pH  adjustment of  the water  was
extremely difficult because of the lack of
buffer capacity in the deionized water; this
unsufficient buffering is why the  equilib-
rium pHs were quite  different from the
initial pHs.
  After 1-L polyethylene bottles were filled
with the radium-spiked water and the cho-
sen weight of activated alumina, they were
placed in a heavy duty tumbler for 7 days
for equilibration at 20' to 25°C. One set of
bottles for  determining one isotherm in-
cluded a blank with no alumina, and five
other bottles contained different  chosen
weights of pH-adjusted alumina. After the
7-day contact period, the suspension was
filtered through a 0.45-n.m membrane fil-
ter before determining the equilibrium pH
         activity of the filtrate.
 Regeneration Experiments
  The spent alumina columns were re-
 generated with 0.5 N HCI followed by 0.25
 N NaOH solutions. The runs had a total
 acid contact time of  45 min and a total
 base contact time of 60 min. Each regen-
 eration effluent bed volume was collected
 separately with the use of a fraction col-
 lector. Eventually, the samples were ana-
 lyzed for pH, ^Ra, and TOG.

 Chemical Analysis
  All ^Ra activity measurements in this
 study were done by the EPA Method 900.1
 (gross radium alpha screening procedure
 for drinking water) described in "Prescribed
 Procedures  for the Measurements of Ra-
 dioactivity in Drinking Water"  (EPA-600/
 4-80/032, August 1980).
   Because we know this method can pro-
 duce falsely high ^Ra results when un-
 wanted  short-lived  alpha emitters  are
 present, we avoided the problem by wait-
 ing typically 21 days to count the samples.
 With proper allowances for the decay of
 short-lived radionuclides, the precision of
 the Method  900.1 analyses for ^Ra was
 ±6% relative standard deviation.
  A Perkin-Elmer Model 5500 Inductively
Coupled Plasma Spectrometer was used
to analyze for barium, calcium, and mag-
nesium.
  A Dionex ion chromatograph measured
sulfate concentration and a  Dohrmann
(Model DC-80)  ultra-low-level TOC ana-
lyzer measured TOC.
  The BaSO4 loading on the BaSO4-im-
pregnated alumina was  analyzed with the
use  of a  hot   alkaline  tetra  sodium
ethylenediammine  tetraacetate (EOTA)
extraction procedure followed by measure-
ment of barium in the extract with the use
of the ICP. This procedure was developed
specifically for this research  because of
the failure of the usual acid digestion pro-
cedures to dissolve the  BaSO4-impreg-
nated alumina.
  The City of Houston, Water Quality Con-
trol Branch, Laboratory Section provided
complete chemical  analysis of the Hous-
ton surface water used in these experi-
ments.

Results and  Discussion

Lemont Field Study Results
  The performance of plain alumina used
to treat the Lemont water was unexpect-
edly good (Figure 1). Based on published
information regarding the poor adsorption
of alkaline-earth cations  at pH  7.2 (the
Lemont water pH), we did not expect any
significant radium removal beyond a few
hundred bed  volumes.  Nevertheless,  we
found that about 3400 BV could be treated
before radium  reached its MCL  (which
corresponded to 3.25 pCi/L ^'Ra and 1.75
pCi/L ^Ra for a total of 5 pCi/L). By way
of explanation, we can  only state that no
previous work has been published on ra-
dium  adsorption onto  activated alumina
and  apparently published  work on mg/L
levels of barium adsorption cannot be ex-
trapolated to pg/L levels  of  radium  ad-
sorption.
  Although plain alumina performed bet-
ter than expected, BaSO4-impregnated alu-
mina  was outstanding  by comparison —
27,500 BV to the radium MCL (Figure 1).
Also  apparent  in Figure 1  is improved
radium removal performance following pe-
riods  of flow  interruption (15 days and 7
days). This suggests that intermittent op-
eration of the alumina column would yield
higher radium loading  and lower radium
concentration in the effluent.  This is  be-
cause stopping  the flow to the column
allows relaxation of the  radium concentra-
tion  gradient in the solid phase,  which,
upon  restarting the flow,  results in a greater
liquid-solid concentration gradient and,
consequently, a  higher radium flux  into
the alumina granules.

Minicolumn Results with
Radium-Spiked Waters
  The minicolumn  runs in the laboratory
with three different feedwaters provided
some hard-to-interpret results. Unlike the
Lemont results, 226Ra-spiked Houston
groundwater produced similar  perfor-
mances for both plain and BaSO4-impreg-
nated aluminas. The plain alumina (12,000
BV) performed somewhat better than did
the BaSO4-loaded variety (10,000 BV) (Fig-
ure 2). The  difference in  alumina perfor-
mance between the Lemont and Houston
groundwaters is probably due to pH. Plain
alumina, as expected, performed better
when the pH was increased to 7.6 to 8.2
compared with the 7.2 pH of the Lemont
water. This agrees with the general obser-
vation that adsorption of cations onto alu-
mina  increases as pH  increases.
  The lower sulfate concentration (17 mg/
L) of the Houston groundwater, compared
with that of the Lemont water (80 mg/L),
may also have contributed to the poorer
performance  of  the BaSO4-impregnated
alumina. For, as we found later, sulfate
concentration is a  major factor in radium
adsorption onto both types of alumina.
  The performance of both types of alu-
mina  on the 226Ra-spiked synthetic water
was dramatically different than the perfor-
mance on  the  Lemont and Houston
groundwaters. We found nearly immedi-
ate breakthrough (500 BV) of radium with
the pH 7.5 to 8.0 synthetic water contain-
ing a  relatively high concentration of barium
(0.9 mg/L) and no  suifate. The poor per-
formance of the aluminas was attributed
mainly to the high level of barium,  an
alkaline earth cation similar to radium in
chemical behavior.
  The performance of the aluminas on
^Ra-spiked Houston  surface  water was,
again, different   from that  on  the
groundwaters and the synthetic water. The
plain  and BaSO4-impregnated aluminas
behaved similarly:  the MCL was reached
at  about 2,000 BV when the feedwater
contained 50 pCi/L of ^Ra. The relatively
good performance  of the plain alumina
was  thought to  be due to the  surface
water's 5 mg/L TOC, which was suspected
of  complexing the  radium  before being
adsorbed by the alumina. For this reason,
additional  minicolumn tests  were per-
formed in which natural organic  matter
TOC was  added  to  resolve the issue.
When 4 mg/L TOC was added to Lemont
groundwater during a  minicolumn test, no
improvement in  radium removal was ob-

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                                                             O BaSO4 Alumina - Run E18
                                                             A Plain Alumina • Run E19
                    Ui
                          0.0
                             0        10000      20000     \ 30000      40000     50000     60000
                                                   Throughput, Bed Volumes
                                                           i         ,      ' ,  ,	    ,      ..       • '.•   . .      : •  .  . •    .   • •:,

 Flgun 1.  Radium removal from Lemont, IL groundwatsr by plain (O.k L) and pressure-impregnated (0.23 L) BaSO.alumina columns. Average influent
          SO/-- 80 mg/L; TOO=0,7 mg/L; Ha2* « 0.2 mg/L; total radium - 15pCi/L; and EBCT=* 3 min. 20,000 BV corresponds to a 42 • day tun length
          ataminEBCT.                                    !
                            0.5
                            0.4
A Plain Alumina-Continuous Flow-Run £15
O SaSQj Alumina*Cont!nuous Flow-Run E16
• BaSO4 Alumina-Intermittent Flow-Run E17
                                         3000         6000\        9000
                                                    Throughput, Bed Volumes
                                     12000
                                                 15000
Flgvr* 2, Radium removal from Ra - 226 - spiked Houston groundw'ater by vacuum impregnated BaSO4 alumina — continuous and intermittent flow.
         Average Influant SO* -17mg/L; 7OC= 0.6 mg/L; Ba**£ 0.02 mg/L; average influent Ra-226=23 pd/L; feed and effluent pH * 7.6 to 8.2; BV
         •• 6.2 mL; and EBCT= 3.3 min. 12,000 BV corresponds to a 28-day run length at 3.3 min EBCT.

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served. Thus, the influence of TOC was
not as significant as suspected.

Statistical Evaluation of Results
  Because of the number of variables in-
volved, the results obtained with column
experiments were  statistically analyzed.
The objective was to establish the effects
of the independent variables, including pH,
feed 22*Ra activity, sulfate, barium,  hard-
ness, and TOC concentrations, on the ad-
sorption of radium onto both  BaSO4-im-
pregnated and plain alumina.
  The analysis was done by means of a
correlation matrix in which an attempt was
made to correlate the dependent variable,
pCi/g radium loading, with the  indepen-
dent variables just mentioned.
  Table 1 summarizes the effects of the
various independent variables on the ra-
dium loadings obtained onto both BaSO4-
impregnated alumina and plain alumina.

Batch Isotherm Studies
  The radium isotherm studies'were done
after the column  experiments in an at-
tempt to obtain a better understanding of
the effects of pH and sulfate  concentra-
tion on radium removal by plain alumina.
  The initial isotherm tests with synthetic
water of variable radium activity were con-
ducted in  glass bottles to  determine the
effect of pH on radium removal.  In these
tests, we observed significant  radium ad-
sorption onto the glass. After correcting
for the influence of radium adsorption onto
the glass, it was clear that, as expected,
the higher the pH the  greater  the radium
adsorption. For example, as pH was in-
creased from 6.8 to 7.9, the radium load-
ing on plain alumina in equilibrium with 5
pCi/L^Ra increased from 100  to 350 pCi/
9-
                                           The results  of the second set of iso-
                                         therms designed to determine the influ-
                                         ence  of sulfate versus chloride as back-
                                         ground  anions are  shown  in  Figure 3.
                                         Polyethylene bottles were used in these
                                         tests  to overcome  the problems caused
                                         by radium  adsorption onto glass. Obvi-
                                         ously, the presence of sulfate dramatically
                                         increased the  adsorption of radium onto
                                         plain alumina. At 5 pCi/L in the water, the
                                         increase in solid phase radium loading is
                                         approximately  four-fold. This verifies the
                                         conclusion  from the  column studies  re-
                                         garding the importance of sulfate.
                                           The mechanism of improved radium up-
                                         take is  thought to  be one  of enhanced
                                         adsorption of neutral RaSOS(J) ion pairs
                                         — the mechanism presumed to be  re-
                                         sponsible for enhanced radium adsorption
                                         onto glass.

                                         Barium in the Column Effluent
                                           There was concern about barium leak-
                                         ing from the BaSO4-impregnated alumina
                                         because a drinking water MCL of 2 mg/L
                                         exists for barium. Thus, the  column efflu-
                                         ents from the Lemont field study and the
                                         lab study were checked for increased
                                         barium. In both the field and lab study, an
                                         increased effluent barium level of approxi-
                                         mately 0.2 mg/L was found.  This was not
                                         considered  serious because it is so far
                                         below the existing 2 mg/L and proposed 5
                                         mg/L  MCLs.

                                         Acid/Base Regeneration of
                                         Alumina
                                           Figure 4 presents the  data from the
                                         regeneration of the plain and BaSO4-im-
                                         pregnated alumina columns, which had
                                         adsorbed approximately equal amounts of
                                         radium. Clearly, the plain alumina is better
                                         regenerated in terms of radium elution
Table 1.   Summary of the Effects* of Various Independent Variables on the Adsorption of Radium
         onto BaSO, - Impregnated and Plain Alumina
    Variable
                             BaSO4 - Impregnated Alumina     Plain Alumina
Feed hardness content
Feed sulfate concentration
Feed barium concentration
Amount BaSo4 loaded
Feed ^Ra activity
Feed TOC concentration
Feed pH
                                          0
                                         ++
                                                                 N/A
0
N/A
     The effects of the independent variables on ^Ra loading were judged as
     significant when R-squared was > 0.1, and F - statistc was > 1.0.
     Causes very significant increase in radium adsorption.
     Causes significant increase in radium adsorption.
     Causes very significant decrease in radium adsorption.
     Not significant.
     Not applicable.
than is BaSO4-impregnated alumina, prob-
ably because of the  difference  in the
mechanism  of  adsorption onto the two
types of alumina. The  hypothesis is that
the major mechanisms of removal of ^Ra
onto plain alumina include the adsorption
of RaSOS( J) ion pairs,  Ra2+-organic  li-
gand complexes, and Ra2* ions. The re-
moval  of radium by BaSO-impregnated
alumina is mainly because Ra2* ions are
incorporated into the BaSO4crystals. While
BaSO4 is being impregnated into the alu-
mina, a fraction  of the plain alumina ad-
sorption sites presumably remains unaf-
fected. Therefore, removal of radium onto
BaSO -impregnated alumina also takes
place by all the mechanisms mentioned
above for plain alumina. The removal  of
radium by plain alumina is a surface phe-
nomenon, whereas  the incorporation  of
radium into the matrix  of BaSO4 crystals
can proceed beneath the  surface. There-
fore,  one  can  expect  radium  to be
desorbable, either by displacement or by
dissolution of the various radium species,
during the acid/base regeneration of plain
alumina. In  the  case of  the BaSO4-im-
pregnated alumina, complete radium  des-
orption can only occur when the BaSO4
dissolves, which is difficult to achieve be-
cause  of its  low solubility.  Removal  of
radium can also occur  by the slow diffu-
sion of radium out of the Ba(Ra)SO4 ma-
trix.
  Another noticeable difference between
the regeneration of  plain  and BaSO4-im-
pregnated alumina is that, whereas all  of
the 226Ra comes off during the acid regen-
eration in the case of the plain alumina, a
significant amount of ^Ra also  comes off
during the base  regeneration in the case
of the BaSO^-impregnated alumina. This
can be explained on the basis of slower
desorption of radium that has been incor-
porated into the BaSO4 crystals. Mass bal-
ances  on radium indicate  about 95%
regenerability of  plain alumina and about
45% regenerability of BaSO4-impregnated
alumina  under  the rather exhaustive
regenerant conditions tested.

Conclusions
  1.  Adsorption onto both BaSO4-im-
      pregnated alumina and  plain  alu-
      mina are technologically attractive
      means to remove radium  from
      small-community water supplies, as
      demonstrated by the long  column
      runs and the high radium loadings
      obtained in field and laboratory stud-
      ies. Radium loadings  of 380'  pCi/
      gm for the BaSO4-impregnated alu-
      mina and 280 pCi/gm for plain alu-
      mina  were obtained  with typical

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                          2000
                           1500
                       t
                       a"
                           1000
                            500
O Control, 0.001 M
A Chloride Background, 0.01 M
m Sulfate Background, 0.005 M
                                                      40         60         80
                                                        Ce, pCi Ra-226/L Water
                                                                                       100
                                                                                                   120
Figure 3.  Isotherms forthe adsorption of Ra-226 onto activated alumina—ionic composition study. Polyethylene bottles were used Equilibrium time was
          7 days and the pH was 6.77.
                          300000
                                                            Plain Alumina - Run R2
                                                           , BaSQd Alumina - Run R1
                                                5              10             15
                                                Throughput, Bed Volumes ofRegenerant
Figure 4,  Regeneration of plain and BaSO4 alumina columns exhausted with Ra-226 spiked Houston surface water. Acid regeneration EBCT= 4.5 min;
          bass regeneration EBCT = 6 min; and regenerant = 11 BVo.SNHCI followed by9BV 0.25 N NaOH.

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    groundwaters containing about 12
    pCi/L of radium.
2.  For the Lemont groundwater with a
    total radium activity  of  18 pCi/L,
    radium  MCL  breakthrough  was
    reached at approximately 25,000
    BV for the fixed-bed process of ad-
    sorption with  BaSO4-impregnated
    alumina. With plain alumina, radium
    MCL breakthrough  was reached
    with a run  length of 12,000 BVwith
    a 23 pCi/L radium-spiked Houston
    groundwater.
3.  The presence  of hardness inhibits
    radium removal onto plain  alumina
    through  direct  competition for ad-
    sorption sites by calcium and mag-
    nesium. Hardness,  in  the range
    found in groundwaters, however, did
    not greatly influence radium removal
    by BaSO4-impregnated alumina be-
    cause the major mechanism of ra-
    dium adsorption  onto  BaSCyim-
    pregnated alumina seemed to be
    the selective exchange of  Ra2* for
    Ba2* ions.
4.  The presence  of sulfate in waters
    enhances radium removal onto both
    types of alumina probably  through
    the formation of RaSO°  ion pairs.
    In batch experiments with plain alu-
    mina, for an equilibrium ^Ra activ-
    ity of 5 pCi/L, approximately 450
    pCi/gm 22
    nated alumina is a direct function
    of the amount of BaSO4 loaded into
    the alumina matrix.
9.  BaSO4-impregnated alumina used
    to adsorb radium is only about 45%
    to  50% regenerable  by acid/base
    regeneration. This  is  because
    BaSO4-impregnated alumina was
    mainly regenerated by extracting
    radium from the highly insoluble
    BaSO., crystals; however, plain alu-
    mina was regenerated by displac-
    ing radium from the  alumina sur-
    face.
10. Plain alumina  used to adsorb ra-
    dium is about 70% to 95%  regen-
    erable through  acid/base regenera-
    tion.  The regeneration efficiencies
    of  plain alumina depended  mainly
    on the characteristics (barium and
    TOO   concentration)   of  the
    feedwater to which the alumina had
    been  exposed. The  presence of
    barium in the feedwater caused a
    decrease in  regeneration efficien-
    cies because of the coprecipitation
    of  radium with BaSO4. The pres-
    ence of TOC  caused part  of the
    226Ra to come  off during the base
    regeneration.
11. The performance of BaSO4-impreg-
    nated alumina or the plain alumina
    depends on  the water chemistry;
    which is the better to use can be
    decided after an in-depth evalua-
    tion of the water chemistry  of the
    water supply in question. Clearly,
    the BaSO4-impregnated  alumina
    performed better with high-hardness
    waters fe 250  mg/L as  CaCO3),
    whereas plain  alumina performed
    equally well or better with low-hard-
    ness waters (< 100 mg/L).
12. In  light of the  above conclusions,
    BaSO4-impregnated alumina  seems
    to  be a good candidate for the ra-
    dium  decontamination  of ion-ex-
    change regeneration brine  solutions
      or other brackish waters. (More
      work, however, needs to be done
      on the effects of calcium and barium
      on  radium adsorption  in  brines.)
      Plain alumina  is probably a better
      choice to remove radium from low-
      hardness well waters, containing >
      40 mg/L sulfate, particularly if the
      regenerability of the alumina is re-
      quired.

Recommendations
  More work is  needed to optimize the
preparation of  BaSO -impregnated alu-
mina. The radium loading capacity of the
BaSO4-impregnated alumina is directly re-
lated to the amount of BaSO4 loaded into
its matrix. Industrial-scale manufacture of
this material will be possible only after the
impregnation process is optimized on a
laboratory-scale.
  Laboratory and field studies should be
done to determine the feasibility of using
the BaSO4-impregnated alumina to decon-
taminate spent ion-exchange brine before
its reuse in processes that would selec-
tively  remove  radium without softening.
Such  processes would (a)  not introduce
sodium into the product water, (b) not use
any salt for regenerant, and (c) not pro-
duce  a brine to  be disposed of into the
sanitary sewer. They would,  however, pro-
duce  a spent  adsorbent media for ulti-
mate disposal.
  More work is needed to clearly identify
the role of metal-ligand complexation on
the adsorption  of  metal ions onto  iron-
oxides as  it pertains  to the radium-alu-
mina system. The role of natural organics
is especially important, and a clear under-
standing of their influence on radium ad-
sorption as related to the molecular size
and component constitution  is necessary.
  The regeneration of both BaSO4-impreg-
nated and plain alumina should be further
studied using  acid and base regenera-
tions.  The primary objectives should be to
determine  (a)  the various desorption
mechanisms involved, (b) the usefulness
of the regenerated media,  (c) the maxi-
mum possible concentrations of radium in
the spent regenerants, and (d) the  pos-
sible means of final  disposal of radium-
contaminated spent regenerant wastewa-
ters.
  The full report was submitted in fulfill-
ment of Cooperative Agreement No. CR-
813148 by the University of Houston un-
der the sponsorship of the  U.S. Environ-
mental Protection Agency.
                                                                    &U.S. GOVERNMENT PRINTING OFFICE: 1992 - 648-080/40241

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   Deepak (?arg and Dennis Clifford are with the University of Houston, Houston, TX
     77204-4791.            •                         '<
   Thomas J. Sorg is the EPA Project Officer (see below).
   TTie complete report, entitled "Removing Radium from Water by Barium Sulfate -
     Impregnated Activated Alumina.11 (Order No. PB92-164 V89/AS; Cost: $19.00;
     subject to change) wilt be available only from:        <
           National Technical Information Service
           5285 Port Royal Road                       '•
           Springfield, VA 22161                       ;
           Telephone: 703-487-4650
   The EPA Project Officer can be contacted at:           I
           Risk Reduction Engineering Laboratory
           U.S. Environmental Protection Agency         <
           Cincinnati, OH 45268                       \
United States
Environmental Protection
Agency
Center for Environmental
Research Information
Cincinnati, OH 4J5268
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Penalty for Private Use $300

EPA/600/SR-92/048

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