United States
                     Environmental Protection
                     Agency
 Air and Energy Engineering
 Research Laboratory
 Research Triangle Park, NC 27711
                    Research and Development
EPA/600/SR-93/020  April 1993
i&EPA       Project Summary
                     Rates  of Reaction and  Process
                     Design  Data for  the  Hydrocarb
                     Process

                    Meyer Steinberg, Atsushi Kobayashi and Yuanki Dong
                      In support of studies for developing
                    the coprocessing of fossil fuels with
                    biomass (wood) by the Hydrocarb pro-
                    cess, experimental and process design
                    data  are  reported. The  experimental
                    work includes the hydropyrolysis of bio-
                    mass and the thermal decomposition
                    of methane in a tubular reactor. The
                    rates of reaction and conversion were
                    obtained at temperature and pressure
                    conditions pertaining to a Hydrocarb
                    process design. A Process Simulation
                    Computer Model was used to design
                    the process and obtain complete en-
                    ergy and mass balances. Multiple feed-
                    stocks were also evaluated, including
                    biomass with natural gas, biomass with
                    coal,  and sewage sludge (SL) and di-
                    gester gas  (DG)  as  additional feed-
                    stocks.
                       This Project Summary was devel-
                    oped by EPA's Air and Energy Engi-
                    neering Research Laboratory, Research
                    Triangle Park, NC, to announce key find-
                    ings of the research project that Is fully
                    documented In a separate report of the
                    same title (see Project Report ordering
                    Information at back).

                    Introduction
                      A feasibility study for the coprocessing
                    of  fossil  fuels  with biomass by the
                    Hydrocarb process was performed for the
                    U.S. EPA (the related report is dated No-
                    vember 1991). Results of the study indi-
                    cated  technical  and economic feasibility
                    compared  to conventional processes for
                    converting  carbonaceous feedstocks such
                    as coal, natural gas, and biomass to clean
                    carbon and methanol fuels. For purposes
                    of mitigating the  global greenhouse car-
                    bon dioxide (CO2) problem, coprocessing
                    fossil fuels with biomass, sequestering all
                    or part of the carbon and using the metha-
 nol mainly as a power or transportation
 fuel, presents the option of reducing and
 eliminating CO  emissions to the atmo-
 sphere while still employing the world's
 fossil fuel resources. The report recom-
 mended that additional  confirmation be
 obtained of the kinetics of the major steps
 in the Hydrocarb process, which includes
 the hydropyrolysis of biomass and the ther-
 mal  decomposition of the  methane-rich
 process gas. To this end, an experimen-
 tal  study  was  undertaken  using  the
 Brookhaven National Laboratory's Tubu-
 lar Reactor Facility.
  In addition to the experimental work, it
 was  recommended that further process
 design  studies be performed employing
 the Process Simulation  Computer Model
 developed by the Hydrocarb Corporation
 with alternative carbonaceous feedstocks.
 This report describes the experimental and
 process design work.
  The report is divided into three sec-
 tions. Part I deals with the hydropyrolysis
 of biomass. Part II deals with the thermal
 decomposition of methane in a tubular
 reactor. Part III gives the results of an
 analysis of the Hydrocarb process with
 alternative and multiple feedstocks.
 Part I.   Hydropyrolysis of Bio-
         mass
  The pyrolysis and hydropyrolysis of bio-
 mass in the form of poplar wood sawdust
 having particle size less than 150 mm in
diameter was investigated in a 25 mm ID
and 2.5 m long tubular reactor facility at
Brookhaven National Laboratory. The tests
were conducted at temperatures  up to
800°C and pressures between 30 and 50
atm.* The experiments were performed in
                                                       * 1 atm = l01.3kPa.


                                                                ^/) Printed on Recycled Paper

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two different  modes, depending  on the
heat-up rate. In the low heat-up rate mode,
the biomass was first loaded in the reac-
tor at room temperature. Hydrogen was
then introduced into the system up to a
desired initial  pressure level. The reactor
was  slowly heated up at a  rate  of less
than 10°C/min. The change  in the pres-
sure in the reactor and the composition of
the effluent gas were monitored with time.
In the higher heat-up rate mode, the reac-
tor was heated up and pressurized with
hydrogen up to the desired reaction con-
ditions before introducing the biomass. The
variations of pressure and gas composi-
tion versus time were then recorded and
analyzed. From these data, rates of reac-
tion and degree of conversion were deter-
mined. A typical run shown in Figure 1
indicates the calculated number of moles
of gas generated as a function of time.
   At low heat-up rate, the reaction pro-
ceeds in two  steps. First pyrolysis takes
place at temperatures of 300 to 400°C
and  then  hydropyrolysis takes place at
700°C and above. This is also confirmed
by experiments  using  pressurized
thermogravimetric analysis. Under condi-
tions of rapid  heat up at higher tempera-
tures and  higher hydrogen  pressure,
gasification and hydrogasification of biom-
ass  is especially effective  in  producing
CO and methane. An overall conversion
of 88 to 90 wt% of biomass was obtained.
This is in agreement with previous  work
on flash pyrolysis and hydropyrolysis of
biomass under rapid heat up  and short
reaction residence time conditions. Initial
rates of biomass conversion  indicate that
the rate increases significantly with  in-
          crease in hydrogen pressure. At 800°C
          and 51.3 atm the initial rate of biomass
          conversion to gases is found to be 92%
          per min.
          Part II.   Thermal Decomposition
                    of Methane
            The reaction rate of methane decompo-
          sition using the same reactor facility was
          investigated in the temperature range of
          700 to 900°C at pressures  ranging from
          28 to 56 atm. In these experiments, meth-
          ane was fed into the reactor  continuously.
          Gas  from upstream and downstream of
          the reactor was analyzed on-line to calcu-
          late the reaction  rate.  The  variations in
          methane concentration vs. residence time
          under different  operating conditions are
          shown in Figure 2. It can be seen from
          the experimental data that the gas resi-
          dence time of about 2 min. is required for
          the reaction to reach near equilibrium com-
          position at 50 aim and 900°C. The rate is
          represented by a conventional model,
                       dCKt
                       ~"dt
kCcm
          where C is the molar concentration and k
          is the rate constant.
            When the initial hydrogen concentration
          is zero, the activation energy for methane
          decomposition is 31.3 kcal/mol,* as deter-
          mined by an Arrhenius Plot. This value is
          lower than for previously published results
          for  methane decomposition  and appears
          to indicate that the high-surface-area sub-
          micron carbon particles found adhering to
          the inside of the reactor tend to catalyze
          the methane decomposition  reaction. The
                                         *  1 kcal.4.l83kJ.
                    10
20         30         40

        Time (min.)
                                                                50
                                                                           60
Figure 1.  Hydropyrolysis of poplar sawdust biomass. The change in number of moles in the reactor
         with time at 800 °C and 52.4 atm of initial hydrogen pressure. Run No. 1152.
rate constant has been found to be ap-
proximately constant at 900°C in the pres-
sure range investigated,  28 to  56 atm.
The rate of methane decomposition  in-
creases with methane partial pressure to
the first order. It is concluded that the rate
of methane decomposition is favored  by
higher temperatures and pressures, while
the thermochemical equilibrium  of meth-
ane decomposition  is favored  by lower
pressures. By extrapolating to higher tem-
peratures, the residence time to reach near
equilibrium at 50 atm would be 41 sec. at
1000°C and 12 sec. at 1140°C.

Part  III.  Design Analysis of the
          Hydrocarb Process with
          Alternate and Multiple
          Feedstocks

  The  design  performance  of the
Hydrocarb  process  with alternative and
multiple feedstocks was investigated. The
alternative feedstocks studied for the
Hydrocarb process included   biomass
(wood), Alaska Beluga coal, Kentucky (bi-
tuminous) coal, North Dakota (lignite) coal,
and Wyodak (subbituminous) coal. A ther-
modynamic-equilibrium-limited  Process
Simulation Computer Model was used to
design the process  and obtain  complete
energy and mass balances. Boundary con-
ditions of pressure, temperature, and mass
balance for the cyclical process  were de-
termined. Two cycles were investigated
depending on whether process gas from
the HPR goes directly to the MPR (cycle
1) or  whether the HPR gas first goes to
the methanol synthesis reactor and con-
denser and then to the HPR (cycle  2).
Cycle 1 produces a higher ratio of metha-
nol to carbon and is preferred. The study
also included using sludge and digester
gas from sewage plants as additional feed-
stocks. It was found that these feedstocks
have to be coprocessed with either biom-
ass or coal to  obtain a workable mass
balance. The effect  of pressure and tem-
perature for both biomass and sludge feed-
stock  was  also investigated.  Carbon
conversion efficiency ranges from 70 to
80% and thermal efficiency between  60
and 80%. Increasing the  HPR and MPR
temperature  improves methanol produc-
tion and thermal efficiency. The methanol
to carbon production rate  decreases with
decreasing system pressure.
   From this study it is concluded that a
most  favorable  operating  conditions  for
coprocessing biomass and methane is 50
atm system pressure, and 900°C for the
HPR and 1000°C for the MPR. Figure 3 is
a complete flowsheet showing  the rates
and compositions of each stream  to and

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from the major pieces of equipment in the
Hydrocarb process for coprocessing bio-
mass (wood) and methane (natural gas).
This process design and the experimental
rate data are being applied to the  design
of reactors for an integrated 22.7  kg/h
Hydrocarb pilot plant.
                                                                                        Equilibrium Data
                                                                                        at 700°Cand56.1 atm
                                                                                                           Equilibrium Data at
                                                                                                           800°C and 56.1 atm
                                                                                                         Equilibrium Data
                                                                                                         at 900°C and 56.1 atm
                                                                20
                                                             40          60          80
                                                                Residence Time (sec.)
                                                                                                                100
                                                                                                                            120
                                                      -0- 900°C 56.1 atm

                                                      -*- 900°C 28.1 atm
                                                                  800°C 56.1 atm
                                                                  900°C41.8atm
                                                                                    700°C 56.1 atm
                                            Figure 2.   Methane concentrations vs. residence time.
                            Hydrocarb Process (Cycle 1)
                                 (Biomass + NG)
                                   (P = 50 atm)
       Wood 4630 kg/h
       NG    694 kg/h
                   *
Char
212 kg/h
                        927 °C
900 °C
2298 kmol/h
CO     6.8
CO
CH
               tf
 0.7
30.1
 6.8
55.7
                         1000°C
       C 1222 kg/h
                                   Off Gas
                                   3 kmol/h
                    CO
                    CO,
                    CHA
                    H.O
                     2.7
                     3.0
                    24.0
                     0.1
                    69.5
                                         50 °C
                                         2167 kmol/h
                                             257 °C
                                   2540 kmol/h
                                   CO     9.2
                                   CO2    0.3
                                   CH.   20.4
                                   H2O    3.7
                                   H.     66.4
                                                  H2O 620 kg/h
        T
       MeOH
       3192 kg/h
260 °C
2304  kmol/h
CO    2.6
CO2   2.8
CH4   22.5
HO    1.6
n     65 4
MeOH 5.1
                                       Carbon Conversion of Feedstock in HPR: 90%
                                       Carbon Efficiency: 72.2%
                                       Thermal Efficiency: 74.9%
Figure 3.   Data summary with wood and CH4 as feedstocks.
                                                                                           'U.S. Government Printing Office: 1993 — 750-071/60224

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  M. Steinberg and A. Kobayashi are with Brookhaven National Laboratory, Upton,
   NY 11973; and Y. Dong is with Hydrocarb Corp., New York, NY 10018.
  Robert H. Borgwardt is the EPA Project Officer (see below).
  The complete report, entitled "Rates of Reaction and Process Design Data for the
   Hydrocarb Process,"(Order No. PB93-155976; Cost: $27.00; subject to change)
   will be available only from
         National Technical Information Service
         5285 Port Royal Road
         Springfield,  VA 22161
         Telephone: 703-487-4650
  The EPA Project Officer can be contacted at
         Air and Energy Engineering Research Laboratory
         U.S.  Environmental Protection Agency
         Research Triangle Park, NC 27711
United States
Environmental Protection Agency
Center for Environmental Research Information
Cincinnati, OH 45268

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