United States
               Environmental Protection
               Agency
Risk Reduction
Engineering Laboratory
Cincinnati, OH 45268
                Research and Development
EPA/600/SR-94/050    April, 1994
EPA       Project Summary
                Cadmium and Chromium
                Recovery from  Electroplating
                Rinsewaters
                Arun R. Gavaskar, Robert F:. Olfenbuttel, and Jody A. Jones
                 This evaluation addresses the prod-
                uct quality, pollution prevention  po-
                tential, and economic factors involved
                in the use of ion exchange to recover
                cadmium  and  chromium from elec-
                troplating rinsewaters and to remove
                contaminants for reuse of rinsewater.
                Cadmium, chromium, and cyanide
                (which is  part  of the cadmium bath)
                are  on EPA's 33/50 list of target
                chemicals. Test results showed that
                the water returned to the rinse after ion
                exchange was of acceptable quality for
                both the cadmium and chromium pro-
                cesses. The  ion exchange resins are
                regenerated  with sodium hydroxide
                (NaOH). On  the cadmium line,  the
                regenerant was subjected  to electro-
                lytic metal recovery (EMR) to recover
                cadmium for reuse in the plating bath.
                On the chromium line, the regenerant
                was  passed through a cation exchange
                resin in an effort to  recover chromic
                acid. Although the  recovery  results
                were good on the cadmium line, chro-
                mic acid could not be recovered in this
                test. The pollution prevention potential
                of ion exchange on the cadmium and
                chromium rinsewater is good; however,
                further testing  is needed to establish
                good recovery  of chromium as chro-
                mic  acid from the regenerant. The ion-
                exchange processes also proved
                economically viable.
                  This Project Summary was developed
                by the U.S. EPA's Risk Reduction En-
                gineering Laboratory (RREL),  Cincin-
                nati, OH, to announce key findings of
                the research project that is fully docu-
                mented in a separate report of the same
title (see Project Report ordering infor-
mation at back).

Introduction
  This study, performed under the U.S.
EPA Waste  Reduction and  Innovative
Technology Evaluation (WRITE) Program,
was a cooperative effort  among EPA's
RREL, the Connecticut Hazardous Waste
Management Service, and the Torrington
Company. The objective of the WRITE
Program is to evaluate, in a typical work-
place environment, examples of prototype
or innovative commercial technologies that
have potential for reducing waste.  The
ion exchange system used in this study
was manufactured by CTEO Tek, Inc.*
and supplied by Plating Services,  Inc.
Other ion exchange  units and technolo-
gies applicable to the same wastestream
(electroplating rinsewaters)  are also
commercially available.
  The objectives of  this study were to
evaluate (1) the effectiveness of the ion
exchange unit in cleaning the rinsewater
for reuse in the rinse tanks, \2.) the pollu-
tion prevention potential of this technol-
ogy,  and (3) the  cost of  ion  exchange
versus the cost of the former practice (dis-
posal).
  Figure  1 shows the cadmium ion ex-
change system configuration. The water
from Rinse 1 tank is  first passed through
a filter to prevent suspended solids from
contacting the resin in the  ion exchange
column. The anionic  resin captures the
cadmium-cyanide complex,  and the water
  Mention of trade names or commercial products does
  not constitute endorsement or recommendation for
                                                                Printed on Recycled Paper

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is returned to the Rinse 2 tank. An emer-
gency bypass valve allows this water to
be discharged to waste in case cadmium
or cyanide levels are found to be too high.
  The resin is periodically regenerated with
a 15 to  20%  NaOH  solution, and  the
regenerant is taken to the electrolytic metal
recovery  (EMR) unit, where cadmium is
recovered on the cathode and returned to
the  plating tank. Some cyanide is  de-
stroyed by decomposition during the EMR
process.
  Figure  2 shows the chromium  system
configuration. The primary ion exchange
resin  is  anionic to remove hexavalent
chrome. In the future, a cationic resin com-
ponent will be added to the primary resin
to remove any trivalent chrome that may
                           be present in the rinsewater. The anionic
                           resin is also regenerated with a 15 to 20%
                           NaOH solution. The resulting solution (so-
                           dium chromate) is run through a second-
                           ary  (cationic) exchange unit that should
                           convert the regenerant back to chromic
                           acid and return it to the plating tank.

                           Product Quality Evaluation
                             The objective of this part of the evalua-
                           tion  was to show  that water  processed
                           through the ion exchange system is clean
                           enough for use as  rinsewater in the cad-
                           mium or chromium  plating lines. Contami-
                           nant-free rinsewater ensures  a good
                           workpiece finish. The approach  was to
                           collect three  samples each  of  the
                           rinsewater, before and after  passing
                                                                     through the ion exchange system. These
                                                                     samples were analyzed in the laboratory
                                                                     to evaluate the removal of contaminants.
                                                                     In addition,  batches  of  rinsewater  (one
                                                                     batch for cadmium and one for chromium)
                                                                     were  spiked with plating bath solution to
                                                                     elevate contaminant  levels (cadmium or
                                                                     chromium), and the spiked rinsewater was
                                                                     run through the ion exchange to test the
                                                                     limits  of the unit. Because rinsewater was
                                                                     continuously  circulated through the ion
                                                                     exchange  system during  the day, three
                                                                     samples of the rinsewater — at the begin-
                                                                     ning,  middle,  and end of  a shift —  were
                                                                     taken to ensure that water quality remained
                                                                     relatively steady over time.
                                                                        Table 1  presents the results of the  labo-
                                                                     ratory analysis of the cadmium rinsewater
        Workpiece	•••-.
             •••..,    .y' Metering  \  ,.-*
                "••. /Pump Make-up \ /

                  '"
   u-JL^JLi         ^_JLr~
—*J  Cadmium   \stiilRin*r           Ri   1   R,
\   I Plating Tank  \(Dragout)  |        \ Rinse 1. j HOT
            Recovered  ป  Emergency Bypass to
            Cadmium   |  Cyanide Wastestream
                                                          Rinse 2
                           L	,	
                  EMR Unit
                                                                     Make-up Water
                                                                           Regenerant
                                                                             Tank
                                                                                        Legend

                                                                                   —*—  Rinse Water
                                                                                   —•ป	  Workpiece
                                                                                   —>.—  Regenerant
                                                     Filter
                                                   Cartridge
 Figure 1. Ion exchange recovery of cadmium from plating rinsewater.
       Workptecet       Catering
               ''•.%  f'" Pump Make-up

                   Chromium
                 I Plating Tank
Recovered
Chromium
                              To Chrome
                              Reduction
                              Wastestream
                                  KVJT
                                                            -+ซ-
                                   Rinse 1 I Rinse 2
               Secondary Catkin
               Exchange
                                                                       Make-up Water
                                                                           Regenerant
                                                                                       Legend

                                                                                   —*— Rinse Water
                                                                                   ••••ป	 Workpiece
                                                                                   —ป— Regenerant
                                                     Filter
                                                   Cartridge
Figure 2. Ion exchange recovery of chromium from plating rinsewater.

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Table 1.  Cadmium Rinsewater Analysis
Sample No.
CD-X1-B1
CD-X1-B2
CD-X1-B3
CD-X1-A1
CD-X1-A2
CD-X1-A3
CD-XS-B1
CD-XS-A1
CD-R1-B1
CD-R1-B2
CD-R1-B3
CD-R2-B1
CD-R2-B2
CD-R2-B3
CD-X30-B1
CD-FB-1
Sample Description
Before ion-x, Run 1
Before ion-x, Run 2
Before ion-x, Run 3
After ion-x, Run 1
After ion-x, Run 2
After ion-x, Run 3
Spike, before ion-x
Spike, after ion-x
Rinse 1, 9:00 am
Rinse 1, 12:30 pm
Rinse 1, 4:00 pm
Rinse 2, 9:00 am
Rinse 2, 12:30 pm
Rinse 2, 4:00 pm
Rinse 1, 30-min
Field blank
pH
11.26
11.41
11.48
11.45
11.51
11.51
NA
NA
10.72
11.37
11.40
11.07
11.50
11.47
11.35
7.50
Conductivity
(umhos/cm)
783
864
936
867
845
885
NA
NA
278
823
985
360
860
970
760
65.3
Cadmium
(mg/L)
7.28
2.23
2.58
0.015
<0.01
0.01
38.7
3.69
1.80
3.55
4.71
0.067
0.105
0.269
4.31
<0.01
Cyanide
(mg/L)
35.60
9.26
13.80
0.037
0.047
0.041
117
14.6
8.55
15.60
24.70
0.28
0.62
1.23
17.60
<0.01
Iron
(mg/L)
0.57
0.22
0.31
0.06
0.06
0.02
NA
NA
0.28
0.34
0.41
0.11
0.07
0.09
0.33
0.21
Dissolved
Solids
(mg/L)
226
196
205
147
161
163
NA
NA
90
190
225
80
164
191
189
50
Suspended
Solids
(mg/L)
1
< 1
< 1
<1
2
<1
NA
NA
1
< 1
10
2
3
<1
3
1
(a) NA = not analyzed.
samples. Most of the cadmium and cya-
nide were removed by ion exchange — in
some cases, to below  detection levels.
The pH of the rinsewater remained steady
at alkaline levels throughout the testing.
   A statistical  t-test (95%  significance
level) was performed based on the aver-
ages and standard deviations of the 1 -min
"before" and "after"  (CD-X1-) data.  Sus-
pended solids levels were very low in both
"before" and "after" samples. After ion ex-
change, concentrations of cadmium, cya-
nide, and iron in the rinsewater decreased
significantly. Overall  dissolved solids lev-
els  also' showed a  significant decrease
after ion exchange;  this indicated a de-
cline in dissolved mass levels. Interest-
ingly,  conductivity  did  not show  any
significant change after ion exchange, in-
dicating that the current-carrying capacity
of the rinsewater did not change. During
ion exchange, heavier ions (cadmium, iron,
etc.) transfer to the  resin and lighter so-
dium ions are  transferred to the water.
Thus,  dissolved mass in the water de-
creases but conductivity remains relatively
constant. Small amounts of fresh makeup
water were added to the rinsewater loop
from time to time to compensate for the
water lost to evaporation and dragout with
the parts; this also helped control conduc-
tivity.
   Table  2  describes the results of the
 laboratory  analysis of the  chromium
rinsewater samples. After ion exchange,
the rinsewater pH levels were slightly al-
kaline  (9.31  to 9.45)  because chromate
ions (and any other contaminant anions)
had been substituted with hydroxide ions.
The  alkaline  pH was neutralized in  the
rinse tanks by the chromic acid residue
on the  parts (workpiece).
  Similar statistical analyses were per-
formed on the chromium data as have
been described for the cadmium data. Sus-
pended solids levels were significantly re-
duced  by the cartridge,.filter ahead  of the
resin. Chromium (total chromium) and iron
levels decreased significantly after ion ex-
change.  Iron removal  may be due  either
to removal of ferrous suspended particles
on the cartridge filter  or fc> (deposition of
complexed iron  on the resin.  As  in  the
cadmium tests, dissolved solids mass de-
creased significantly, but conductivity (cur-
rent-carrying  strength) remained constant
after  ion exchange.  This  is  because
heavier chromates in the rinsewater were
replaced with lighter hydroxide ions.

Pollution Prevention Evaluation
  The pollution prevention potential of the
ion exchange technology was assessed
in terms of  waste volume reduction  and
pollutant reduction. Waste volume  reduc-
tion addresses  the gross wastestream
(e.g., Ib  of wastewater treatment sludge)
and affects environmental resources (e.g.,
landfill space) expended through disposal.
Pollutant reduction addresses the specific
pollutants in the wastestream (e.g., chro-
mium in the sludge).
  Table 3 summarizes the waste volume
reduction. By using ion  exchange, large
volumes of water are saved from going to
waste. This water (an important resource)
can be reused as  a rinse on the cadmium
and chromium lines. Without ion exchange,
Torrington  must maintain high rinsewater
flow rates  (8 gpm for the cadmium  line
and 2 gpm for the chromium line). These
continuous flows generate large amounts
of wastewater that have to  be treated on
site. With the ion exchange system on the
cadmium line, Torrington requires only 50
gal/day  to make up for dragout  losses. A
similar makeup rate is expected  on the
chromium  line.  Therefore, with  the addi-
tion  of  the ion-exchange  system,  the
amount of wastewater that must be treated
is reduced. Virtually eliminating the waste-
water stream also eliminates the hazard-
ous  sludge (containing  cadmium  or
chromium) that has to be handled, trans-
ported,  and disposed.
  In terms of pollutant  reduction on the
cadmium line, the  pollutants of interest
are cadmium and cyanide. Before ion ex-
change, cadmium in the rinsewater was
lost to wastewater, which was sent to an
on-site  wastewater treatment plant.  The
wastewater was treated in a steel cyanide

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Tablt>2. Chromium Rinsewater Analysis
Sample No.
CR-X1-B1
CR-X1-B2
CR-X1-B3
CR-X1-A1
CR-X1-A2
CR-X1-A3
CR-XS-B1
CR-XS-A2
CR-X2-B1
CR-FB-1
Sample Description
Before ion-x, Run 1
Before ion-x, Run 2
Before ion-x, Run 3
After ion-x, Run 1
After ion-x, Run 2
After ion-x, Run 3
Spike, before ion-x
Spike, after ion-x
Rinse 1, 30-min
Field blank
PH
4.83
4.67
4.41
9.38
9.31
9.45
NA(a)
NA
4.68
7.50
Conductivity
(umhos/cm)
103
104
106
198
126
115
NA
NA
105
65.3
Total
Chromium
(mg/L)
20.0
18.2
21.3
0.048
0.111
0.271
33.6
0.294
19.9
0.04
Iron
(mg/L)
0.90
0.85
0.87
0.15
0.20
0.26
NA
NA
0.73
0.21
Dissolved
Solids
(mg/L)
93
99
106
96
70
71
NA
NA
87
50
Suspended
Solids
(mg/L)
9
8
6
<1
<1
< 1
NA
NA
2
1
(a) NA " Not analyzed.
Tablo 3. Waste Volume Reduction
             Without Ion Exchange
            With Ion Exchange
Waste
Description
Cadmium System
Wastewater
Chromium System
Wastewater
Amount
Generated per
Yearฎ
1,920,000 gal
480,000 gal
Waste
Description
Wastewater
Regenerant
Fitter cartridges
Wastewater
Regenerant
Filter cartridges
Amount
Generated per
Yearฎ
Ogal
660 gal
6
Ogal
840 gal
12
(a) Based on values of 16 hr/day, 5 days/wk, 50 wk/yr.
(b) Based on pilot tests conducted by the Torrington Company and resin capacity.
treatment tank using chlorine gas, sodium
hypoohlor'rte, calcium hypochlorite, and
NaOH to oxidize the cyanide. The cad-
mium and  other  metals  formed hydrox-
ides that settled in the clarifier as sludge,
which was then hauled  off site for dis-
posal. The  treated water was discharged
to the municipal sewer under a permit.
  At Torrington, prior to ion exchange,
approximately 69 Ib of cadmium,and 281 Ib
of cyanide were discharged annually. Now,
because most of  the cadmium can be
recovered  and reused,  this pollutant is
virtually eliminated from the wastestream.
Some cyanide  is  also destroyed  in the
cadmium recovery process.
  On the chromium  line, without ion ex-
change, approximately 80 Ib of chromium
Is discharged annually. With ion exchange,
most of the chromium will be captured on
the resin, which  will  be regenerated with
NaOH. The  regenerant then will  pass
through a cation exchange resin for con-
version of sodium chromate to chromic
acid. However; when this  recovery was
performed during the pilot unit testing, the
final regenerant liquid still showed a pH of
13.08. This indicates that  sodium chro-
mate had not been converted to chromic
acid; if it had been,  the pH would  have
been much lower. This  may be  because
(a) an excess of NaOH was used to re-
generate the  resin and/or  (b) insufficient
resin was available  to  exchange all the
.sodium in the regenerant. Further testing
is needed to  determine the feasibility of
the chromic acid recovery process.

Economic Evaluation
   The economic evaluation involves com-
paring the costs of the ion  exchange op-
eration with those of the former practice
(counterflow rinse). These comparisons are
summarized in Tables 4 and 5. Operating
costs for ion exchange recovery are much
lower than those  for  counterflow rinse
alone. The main cost saving is the reduc-
tion in Wastewater treatment costs.
  In addition to operating cost savings,
the recovered cadmium has value because
it is reused in the plaiting bath as a cad-
mium anode. The  cost of cadmium  an-
odes is approximately $15/lb. The resulting
value of the 69 Ib/yr of recovered cad-
mium is approximately $1,036/yr.
  The chromium deposited on the ion ex-
change  resin also  has value if it can be
successfully recovered as chromic acid.
The cost of chromic acid is approximately
$2.50/lb. Approximately 80 Ib/yr of chro-
mium metal is  deposited on the ion  ex-
change  resin. This corresponds to about
154lb of chromic acid (CrO3). However,
further testing is needed to establish  the
feasibility of chromic acid recovery from
the chromium in the regenerant.
  The purchase price of the cadmium ion
exchange system was $8,100 (including
ion exchange resin column,  pumps, and
collection  tanks). The  EMR equipment
price was $4,125 (including rectifier, pump,
anodes, cathodes,  and solution tank). In-
stallation cost at Torrington, including ma-
terials  (piping, etc.)  and  labor, was
approximately $3,500, to which $5,000 was
added to approximate the cost of in-house
pilot testing to determine specifications for
the individual plant.
  The purchase price of the chromium ion
exchange system is estimated to be $8,200
(including  ion  exchange  resin column,
pumps,  and  tanks). Installation  cost at
Torrington  is expected to  be $3,500, in-
cluding  materials '(piping, etc.)  and labor.

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Table 4. Operating Costs Comparison for Cadmium System
Item
  Amount
   Used
  per Year
                                                   Unit
                                                   Cost
                       Total Annual
                          Cost
Without Ion Exchange

    Freshwater
    Wastewater treatment

With Ion Exchange

    Freshwater
    Chemicals (50% NaOH)
    Energy
    Labor
        i
    Routine maintenance
    - filter cartridges
    - EMR anode plates
    - EMR cathode plates
    - labor

    Waste Disposal
    - regenerant
    - filters
1,920,000 gal
1,920,000 gal
 12,500 gal
   96 gal
 1564 kWhr
   173hr
     6
     1
     12
   24 hr
   660 gal
     6
$0.70/1000 gal
 $22/1000 gal
            Total
$0.70/1000 gal
  $ 1.50/gal
 $ 0.075/kWhr
    $7/hr
     $5
     $30
     $30
    $7/hr
 $22/1000 gal
 $ 400/36 units
                                                         Total
 $ 1,344
$42,240
$ 43,584
     $9
  $144
  $117
 $ 1,211
    $30
    $30
   $360
   $168
    $15
    $67
 $ 2,151
 Table 5. Operating Costs Comparison for Chromium System
Item
  Amount
    Used
  per Year
                                                   Unit
                                                   Cost
                       TotalAnnual
                          Cost
 Without Ion Exchange

     Freshwater
     Wastewater treatment
 With Ion Exchange
 480,000 gal
 480,000 gal
     Freshwater           12,5.00 gal
     Chemicals (50% NaOH)   240 gal
     Energy               1492kWhr
     Labor                  149 hr
$ 0.70/1000 gal
 $15/1000 gal
            Total
                      $0.70/1000 gal
                         $ 1.SO/gal
                        0.075/kWhr
                          $7/hr
   $336
  $7,200
  $7,536
                              $9
                            $360
                            $112
                           $ 1,043
Routine maintenance
- filters
- labor '
Waste Disposal
- regenerant
- filters


12
24
840 gal
6


$5
$7/hr
$15/1 000 gal
$ 400/36 units
Total

$60
$168
$13
$67
$ 1,832
 The approximate  cost  of $5,000 for in-
 house testing was also added for this unit.
   A rough estimate of the payback period
 can be obtained by the following formula:
 Payback, years =
                      capital costs
                   operating cost savings
                    + recovery value
   Therefore, the payback period for the
 cadmium ion exchange system is less than
                   1 year. For the chromium system, the pay-
                   back period is approximately 3 years. Be-
                   cause  chromic acid  recovery from  the
                   regenerant-is yet to  be  established,  no
                   recycled chromium value is assumed.
                     The above payback period estimation is
                   a simple calculation that  (does  not take
                   into account such factors as> taxes, depre-
                   ciation, inflation, etc. A more detailed eco-
                   nomic evaluation, based on Ithe worksheets
 provided  in the Facility Pollution Preven-
 tion Guide (EPA 600/R-92/088), was per-
 formed that took these factors into account.
 The results showed that, for the cadmium
 process,  the  return on  investment (with
 cost of capital equal to 15%) was still less
 than  1 year. For the chromium process,
 the return on investment (with cost of capi-
 tal equal  to 15%) was over 5 years. This
 includes  capital costs of engineering and
 installation as well as increased overhead
 costs due to addition of the units.

 Conclusions and  Discussion
   The evaluation showed that rinsewater
 on both cadmium and chromium lines at
 Torrington Company can be reused after
 subjecting it to filtration and ion exchange
 to remove  impurities. Large  volumes of
 water are thus saved,  and large amounts
 of hazardous metals sludge are kept from
 the environment. The  sidestreams from
 ion exchange are negligible compared with
 the wastewater and sludge wastestreams
 that are generated in the absence of ion
 exchange. The ion exchange resin can be
 regenerated with NaOH. On the cadmium
 line, the  regenerant can be subjected to
 EMR  and the cadmium recovered on the
 cathode.  This electrode, with the depos-
 ited cadmium, is then inserted in the plat-
 ing tank  as a cadmium anode. Thus, a
 hazardous  pollutant, cadmium,  is reused.
 On the  chromium line, further testing  is
 needed to  establish the feasibility of  re-
 covering  chromium as  chromic acid  for
 reuse in  the bath.
    Without  ion exchange, the rinsewater
 must  undergo an  expensive wastewater
 treatment process. The cost of operating
 the ion exchange unit is more than offset
 by the savings  in wastewater treatment
 costs and by the value of the  recovered
 product.  In addition to the direct economic
 benefits, the ion exchange system also
 reduces  Torrington Company's potential
 liability by virtually eliminating the risks
 involved  during off-site transport and dis-
 posal of  hazardous sludge.
    The full  report was  submitted in fulfill-
• ment of  Contract  No.  68-CO-0003, Work
 Assignment No. 3-36, by Battelle under
 the sponsorship of the U.S. Environmen-
 tal Protection Agency.
                                                                         •A-U.S. GOVERNMENT PRINTING OFFICE: 1994 - 55WW7/80Z22

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Awn R. Gavaskar, Robert F. Olfenbuttel, andJodyA. Jones are with Battelle
  Memorial Institute, Columbus, OH 43201-2693
Lisa Brown Is the EPA Project Officer (see below).
The complete report, entitled "Cadmium and Chromium Recovery from
    Electroplating Rinsewaters," (OrderNo. PB94-156395; Cost: $19.50,
    subject to change) will be available only from:
        National Technical Information Service
        5285 Port Royal Road
        Springfield, VA 22161
        Telephone: 703-487-4650
The EPA Project Officer can be contacted at:
        Risk Reduction Engineering Laboratory
        U.S. Environmental Protection Agency
        Cincinnati, OH 45268
   United States
   Environmental Protection Agency
   Center for Environmental Research Information
   Cincinnati, OH 45268

   Official Business
   Penalty for Private Use
   $300
     BULK RATE
POSTAGE & FEES PAID
         EPA
   PERMIT No. G-35
   EPA/600/SR-94/050

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