United States
               Environmental Protection
               Agency
Air and Energy Engineering
Research Laboratory
Research Triangle Park, NC 27711
               Research and Development
EPA/600/SR-94/126  November 1994
EPA       Project  Summary
               Evaluation  of  Containment  and
               Control Options  for Methyl
               Bromide  in  Commodity
               Treatment
              Glenn B. DeWolf and Matthew R. Harrison
                Methyl bromide (MeBr) is an ozone-
              depleting chemical scheduled  to  be
              phased out by The Clean Air Act by the
              year 2001. For agricultural  commodity
              fumigation, there is no ready substi-
              tute  for MeBr. This study was under-
              taken to investigate means for MeBr
              recovery, reuse, and destruction to pre-
              vent atmospheric emissions if its lim-
              ited use were still allowed.
                Approximately 4-5 million  Ib/yr
              (1.8  - 2.3 million kg/yr) of MeBr is
              used for  commodity/agricultural
              harvest fumigation. Commodity  fu-
              migation is carried out extensively at a
              few locations, mostly major seaports.
              Fumigation is conducted in chambers
              built for holding the commodity during
              fumigation and in temporary enclosure,
              such as under tarpaulins  and  in ve-
              hicles. The emissions are vented to the
              atmosphere.
                Few control systems exist for MeBr
              emissions. Likewise,  control system
              research and  development has  been
              limited. Vendors have  proposed con-
              trol technologies for MeBr  control,  re-
              covery, and recycle, but few systems
              have been built. Conventional  vapor
              control technologies, such as activated
              carbon adsorption systems, appear to
              be applicable to MeBr emissions. These
              systems must also provide for recov-
              ery. Control will probably be expensive
              due to the small volumes  of recover-
              able material and the intermittent na-
              ture of fumigation operations.
                This Project Summary was developed
              by EPA's Air and Energy Engineering
              Research Laboratory,  Research  Tri-
              angle Park, NC, to announce key find-
ings of the research project that is fully
documented in a separate report of the
same title (see Project Report ordering
information at back).

Introduction
  Methyl  bromide (MeBr), with  the
chemical  formula CH3Br, also  called
bromomethane,  is  listed by the 1991
Montreal Protocol as  an ozone deplet-
ing chemical similar to the other haloge-
nated  hydrocarbons  such as  the
chlorofluorocarbons  (CFCs). The U.S.
Environmental Protection Agency's (EPA's)
regulations authorized by the Clean Air
Act  (CAA) call for a phaseout of MeBr
production by the year 2001. This would
mean an end to uses of MeBr where the
material is emitted to the atmosphere since
no future supply of MeBr would be avail-
able. In some applications, there is no
apparent, ready substitute for MeBr. There-
fore, this study was undertaken to investi-
gate possible means for MeBr recovery
for reuse and for MeBr destruction to pre-
vent atmospheric emissions if its limited
use were still allowed.
  MeBr is widely used in U.S. agriculture
as a fumigant. A fumigant is a  material
that  can exist as a gas in a concentration
lethal to a pest organism. As a gas, it can
penetrate  the material  being  fumigated,
and then diffuse away after the fumigation
ends. MeBr is a very useful general fumi-
gant since it is a permeating gas at ambi-
ent temperatures and pressures and since
it has  a very desirable toxicity to many
pest populations.
  Table 1  shows that the primary use of
MeBr is in soil fumigation, where it is used
to kill nematodes and soil insects prior to

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Table 1.   Methyl Bromide Use [million Ib/yr (million kg/yr)]

                          1991 Use from CPS
                                                 1990 Use from NAPIAP
Total
Soil Fumigation
Chemical Intermediate
Structural Space Fumigation
Commodity Space Fumigation
47
35
3.8
3.8
3.8
(21)
(16)
(1.7)
(1.7)
(1.7)
64
47

4 to 9
5
(29)
(21)

(1.8 to 4.1)
(2.3)
planting. According to Chemical Products
Synopsis (CPS),  approximately 75%  of
the 47 million  Ib (21  million kg) of MeBr
consumed in 1991 in the U.S. was for this
application. An additional 8% of MeBr con-
sumption is as a chemical intermediate or
as a solvent. The remaining 16% of MeBr
consumption is used  in  space  fumigation.
Half of that space fumigation is structural
fumigation,  and half is  for commodity fu-
migation.
  The National Agricultural Pesticide Im-
pact Assessment Program (NAPIAP)  of
the U.S. Department of Agriculture (USDA)
has produced use numbers for MeBr that
are different from the CPS numbers. How-
ever,  both  sources  show that approxi-
mately 4-5 million Ib/yr (1.8 - 2.3 million
kg/yr)  of MeBr is used  for commodity/
agricultural  harvest space fumigation.
  This study has gathered preliminary data
that can be used to determine if some of
the essential agricultural commodity fumi-
gation applications of MeBr could be con-
tinued by the use of some emission control
methods on those commodity  fumigation
applications.

Conclusions

MeBr Uses and Quantities
  Since MeBr uses are relatively restricted,
MeBr can be viewed  as a specialty fumi-
gant.  The consumption  of MeBr for space
fumigation  of  commodities  represents
about 8% of MeBr use. The primary use
for  MeBr in commodity fumigation  is for
fruits  and nuts. In the treatment of these
commodities, there are  general commod-
ity  containment schemes  that are com-
mon  throughout the industry,  although
some details  may vary  with individual in-
stallations. The types of configurations for
commodity  containment are relatively lim-
ited.
  Fumigation is carried  out extensively at
a few primary locations,  mostly major sea-
ports. Two of the largest ports where MeBr
is used are San Diego  and Philadelphia.
Other major ports include Seattle and Mi-
ami, but any port where fruit and nuts are
imported is a candidate. Also, fumigation
facilities  are  reported to be  present  at
some airports and military facilities.

Emission Source
Characteristics
  Emissions sources are characterized in
terms of physical configuration and  emis-
sion stream characteristics.
  Physical configurations are divided into
two categories: (1)  sources with a duct,
pipe, or stack outlet, and (2) sources with
multiple,  irregular outlets. The former oc-
cur in chambers specifically built for hold-
ing  the commodity during fumigation. The
latter occur  with tarpaulin  fumigation  or
fumigation in vehicles where ordinary leak-
age or simply an open  door is used  to
vent the MeBr when fumigation is com-
plete.
   The emissions arise when air is blown
through  the commodity to  remove the
MeBr. Currently the  emissions are vented
directly to the atmosphere.
  Little  data  are  currently  available for
stream characteristics. Information that is
available suggests flow rates in the  range
of no more than a few thousand to  a few
tens of thousand of cubic feet per minute
air flow with  a  MeBr content ranging from
a few hundred to a few thousand parts
per million.
  Currently few control systems exist for
MeBr emissions. Likewise, research and
development related to control system de-
sign has been  extremely limited.
  Various vendors have  proposed control
technologies for MeBr control, recovery,
and recycle. Few systems have been built.
Currently, systems are being investigated
and the Port of San Diego is installing a
MeBr treatment system. Some systems
have  been  installed overseas.  Technical
details of these systems are not readily
available, so that  further work would be
required to determine how extensively they
control emissions and how effective they
may be  at recovery.
  In general, conventional vapor control
technologies, such  as  activated carbon
adsorption systems,  appear  to be  appli-
cable to MeBr emissions. However,  in the
context  of minimum or even  zero  emis-
sions, depending  on the  regulatory sce-
nario, control systems must also provide
for  recovery. Conventional  approaches
using condensation and  other  methods
appear to be applicable here.  The funda-
mental technologies  required appear to
exist, but the specifics of the application
of these technologies to the MeBr control
issue require much more investigation and
design data acquisition.

Process Economics
  Process economics of MeBr control and
recovery are not well  defined. Scattered
data on  actual and possible costs of sys-
tems were skimpy. Because many com-
ponents of a control system would appear
to rely on existing technologies, costs and
the  corresponding  economics do not ap-
pear to be difficult to estimate. Costs can
be expected  to be comparable to those of
other vapor  control systems for similar
gas stream flow rates.
  Preliminary economics of a conceptual
design prepared specifically for this  report
indicate  that control will be relatively ex-
pensive.  The relative expense compared
with  control  systems of similar nature in
other applications  is based on  relatively
small volumes of recoverable material that
would be handled  and  the intermittent na-
ture  of many of the fumigation operations
to which the  control system would be ap-
plied. At  this time,  sufficient data are not
available for either design or costs to make
a definitive statement.
   A factor that might considerably influ-
ence the economics of MeBr control is the
availability of future MeBr supplies. This
will  be influenced  by the  regulatory sce-
nario. A  total ban, but allowance of the
use  of existing MeBr inventories  with re-
cycle would,  in effect, make recycle  im-
practical  for  technical  reasons. Chemical
reaction losses would  quickly deplete the
supply.  On  the other hand, a  selective
ban  that would allow  some manufacture
of MeBr  to  continue might drive up  the
price, assuming a  manufacturer were will-
ing to continue manufacture, because the
use  volume  would  be sharply  reduced.
Unit  manufacturing costs  would increase
sharply.

Current Research and
Development Activities
  Current research and development ac-
tivities appear to be underway in several
quarters on the very issues discussed in
this report. These activities do appear to

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be limited at the present time,  however.
Much of the current work appears to  be
under the auspices of various vendors of
systems and  equipment.  Some govern-
ment agencies and industrial groups are
showing  increasing interest in funding
some research. The United Nations Envi-
ronment Programme (UNEP) has had a
leading role in addressing some of these
issues.
Information Gaps

  In general, information is lacking in two
fundamental categories:  (1) MeBr emis-
sion source characterization and (2) con-
trol technology  characterization. The
fundamental focus needs to shift  beyond
mere  reduction of emissions and toward
recovery and recycle. There also needs to
be an effort to gather some fundamental
performance data related specifically to
fundamental stream characteristics. This
is especially important because of the re-
ported  potential for the accumulation of
various commodity chemical components
picked  up by the MeBr on each cycle of
contact with the commodity  being fumi-
gated.  Detailed economic evaluations
based on existing data should be carried
out early in order to better direct the re-
search  and maximize research efficiency.

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   G. DeWolfand M. Harrison are with Radian Corp., Austin, TX 78720-1088.
   Robert V. Hendriks is the EPA Project Officer (see below).
   The complete report, entitled "Evaluation of Containment and Control Options for
     Methyl Bromide in Commodity Treatment," (Order No. PB94-195070; Cost:
     $27.00, subject to change)  will be available only from:
           National Technical Information Service
           5285 Port Royal Road
           Springfield, VA22161
           Telephone: 703-487-4650
   The EPA Project Officer can be contacted at:
           Air and Energy Engineering Research Laboratory
           U.S. Environmental Protection Agency
           Cincinnati, OH 45268
United States
Environmental Protection Agency
Center for Environmental Research Information
Cincinnati, OH 45268

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         EPA
   PERMIT No. G-35
EPA/600/SR-94/126

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