vvEPA
 I
 I
o
                   United States
                   Environmental Protection
                   Agency
             Region 7
             324 East Eleventh St.
             Kansas City, Mo. 64106
                   Air
EPA 907/9-81-008
OctoL 1981
                                           EPA REGION VII IRC
                                            160442
Emission Test Report

Prestolite Lead
Acid Battery Plant
Manchester, Iowa

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                                                SEP
                                                   1 6 1982
              EMISSION TEST REPORT

        PRESTOLITE LEAD ACID BATTERY PLANT
                 MANCHESTER, IOWA
                   Prepared by

            PEDCo Environmental, Inc,
               11499 Chester Road
             Cincinnati, Ohio  45246
             Contract No. 68-02-3512
             Work Assignment No. 17
                   PN 3525-17
               EPA Project Officer
              Mr. DeWayne E. Durst
      U.S. ENVIRONMENTAL PROTECTION AGENCY
                   REGION VII
AIR AND HAZARDOUS MATERIALS DIVISION  (ARHM/ANRB)
        AIR, NOISE, AND RADIATION BRANCH
              324 EAST 11TH STREET
          KANSAS CITY, MISSOURI  64106
                   October 1981

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                                DISCLAIMER
     This report was furnished to the Environmental Protection Agency
by PEDCo Environmental, Inc., 11499 Chester Road,  Cincinnati,  Ohio 45246,
in fulfillment of Contract No. 68-02-3512,  Work Assignment No. 17.  The
contents of this report are reproduced herein as received from PEDCo
Environmental, Inc.   The opinions, findings, and conclusions expressed
are those of the author and not necessarily those of the Environmental
Protection Agency.   Mention of company or product names is not to be
considered as an endorsement by the Environmental Protection Agency.
                                    11

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                            CONTENTS
Figures
Tables
Quality Assurance Element Finder

1.   Introduction                                           1-1

2.   Project Summary                                        2-1

3.   Process Operation                                      3-1

     3.1  Process description                               3-1
     3.2  Environmental control devices tested              3-17
     3.3  Process data                                      3-18

4.   Sample Locations and Test Methods                      4-1

     4.1  Barton oxide process baghouses No.  1 and No.  2    4-1
     4.2  Entoleter scrubber outlet                         4-3
     4.3  Baghouse No. 1                                    4-5
     4.4  Baghouse No. 2                                    4-5
     4.5  Baghouse No. 3                                    4-7
     4.6  Carter-Day baghouse                               4-8
     4.7  Velocity and gas temperature                      4-8
     4.8  Molecular weight                                  4-8
     4.9  Particulate matter                                4-10
     4.10 Lead                                              4-10

5.   Summary of Results                                     5-1

     5.1  Barton oxide process baghouses                    5-2
     5.2  Entoleter scrubber outlet                         5-7
     5.3  Baghouse No. 1 outlet                             5-11
     5.4  Baghouse No. 2 outlet                             5-12
     5.5  Baghouse No. 3 outlet                             5-16
     5.6  Carter-Day baghouse outlet                        5-20

6.   Quality Assurance                                      6-1
                                111

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Appendix A



Appendix B



Appendix C



Appendix D



Appendix E



Appendix F



Appendix G
       CONTENTS (continued)



                                             Page




Computer printout and sample calculations    A-l




Field data                                   B-l



Laboratory results                           C-l



Sampling and analytical procedures           D-l



Calibration procedures and results           E-l



Quality assurance summary                    F-l



Project participants and activity log        G-l
                               IV

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                             FIGURES

Number                                                      Page
 3-1      Process Flow Diagram for the Production of
            Antimony Lead Alloy Batteries                   3-2

 3-2      Process Flow Diagram for the Production of
            Calcium Lead Alloy Batteries                    3-3

 4-1      Barton Oxide Process and Secondary Baghouse
            Outlet                                          4-2

 4-2      Entoleter Scrubber Outlet                         4-4

 4-3      Baghouses No. 1, 2, and 3 Sample Locations        4-6

 4-4      Carter-Day Baghouse Sample Location               4-9

 6-1      Audit Report Sample Meter Box                     6-7

 6-2      Audit Report Sample Meter Box                     6-8

 6-3      Audit Report Sample Meter Box                     6-9

 6-4      Audit Report Sample Meter Box                     6-10

 6-5      Audit Report Sample Meter Box                     6-11

 6-6      Audit Report Sample Meter Box                     6-12

 6-7      Audit Report Sample Meter Box                     6-13

 6-8      Audit Report Sample Meter Box                     6-14

 6-9      Audit Report Sample Meter Box                     6-15

 6-10     Audit Report Digital Indicator                    6-16

 6-11     Audit Report Digital Indicator                    6-17

 6-12     Audit Report Digital Indicator                    6-18
                                .v

-------An error occurred while trying to OCR this image.

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                        TABLES (continued)

Number                                                      Page

 3-10     Calculated Production Data for the Wrapping
            Process and Intercell Line 2 During Each
            Sample Run                                      3-32

 3-11     Production Data for the Calcium Battery MAC
            Machines and Inspection Stations Calculated
            During Each Sample Run                          3-32

 5-1      Summary of Flue Gas Conditions at Barton Oxide
            Baghouse Outlets                                5-3

 5-2      Summary of Lead and Particulate Emissions at
            Barton Oxide Process Baghouses (Metric Units)    5-4

 5-3      Summary of Lead and Particulate Emissions Data
            at Barton Oxide Process Baghouses (English
            Units)                                          5-5

 5-4      Summary of Flue Gas Conditions at Entoleter
            Scrubber Outlet                                 5-8

 5-5      Summary of Lead and Particulate Emissions Data
            Entoleter Scrubber Outlet (Metric Units)        5-9

 5-6      Summary of Lead and Particulate Emissions Data
            Entoleter Scrubber Outlet (English Units)       5-10

 5-7      Summary of Flue Gas Conditions at Baghouse No. 1
            Outlet                                          5-13

 5-8      Summary of Lead and Particulate Emissions Data
            at Baghouse No. 1 Outlet (Metric Units)         5-14

 5-9      Summary of Lead and Particulate Emissions Data
            at Baghouse No. 1 Outlet (English Units)        5-15

 5-10     Summary of Flue Gas Conditions at Baghouse No. 2
            Outlet                                          5-17

 5-11     Summary of Lead and Particulate Emissions Data
            at Baghouse No. 2 Outlet (Metric Units)         5-18

 5-12     Summary of Lead and Particulate Emissions Data
            at Baghouse No. 2 Outlet (English Units)        5-19

 5-13     Summary of Flue Gas Conditions at Baghouse No. 3
            Outlet                                          5-21
                                VI1

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                        TABLES (continued)

Number                                                      Page
 5-14     Summary of Lead and Particulate Emissions Data
            at Baghouse No. 3 Outlet (Metric Units)         5-22

 5-15     Summary of Lead and Particulate Emissions Data
            at Baghouse No. 3 Outlet (English Units)        5-23

 5-16     Summary of Flue Gas Conditions at Carter-Day
            Baghouse Outlet                                 5-25

 5-17     Summary of Lead and Particulate Emissions Data
            at Carter-Day Baghouse Outlet (Metric Units)    5-26

 5-18     Summary of Lead and Particulate Emissions Data
            at Carter-Day Baghouse Outlet (English Units)   5-27

 6-1      Field Equipment Calibration                       6-3

 6-2      Dry Gas Meter Audits                              6-6

 6-3      Audit Report Lead Analysis                        6-20
                               Vlll

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                QUALITY  ASSURANCE  ELEMENT  FINDER
(1)   Title  page

(2)   Table  of  contents

(3)   Project description

(4)   Project organization and  responsi-
     bilities

(5)   QA  objective  for measurement  data
     in  terms  of precision,  accuracy, com-
     pleteness, representativeness and
     comparability

(6)   Sampling  procedures

(7)   Sample custody

(8)   Calibration procedures  and frequency

(9)   Analytical procedures

(10)  Data  reduction, validation,  and
     reporting

(11)  Internal  quality control  checks and
     frequency

(12)  Performance and system  audits and
     frequency

(13)  Preventive maintenance  procedures  and
     schedules

(14)  Specific  routine procedures  used
     to  assess data precision,  accuracy and
     completeness  of specific  measurement
     parameters involved

(15)  Corrective action

(16)  Quality assurance  reports to management
                                                   Location
                                               Section     Page
             11

   1        1-1


Appendix F  F-3
Appendix F  F-3

Appendix D  D-l

Appendix C  C-l

Appendix E  E-l

Appendix D  D-l


Appendix F  F-4


Appendix F  F-5


Appendix F  F-4


Appendix F  F-6
Appendix  F  F-5

Appendix  F  F-6

Appendix  F  F-7
                                ix

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                            SECTION 1



                          INTRODUCTION






     The U.S. Environmental Protection Agency (EPA) established




lead as a criteria pollutant in the October 5, 1978, Federal



Register (43 FR 46246).   The Clean Air Act, as amended in 1977



(the Act),  required each state to submit a State Implementation



Plan (SIP)  demonstrating attainment of the National Ambient Air




Quality Standard  (NAAQS) for lead by October 30, 1982, or if



granted a time extension by EPA, by October 30,  1984.  The infor-



mation contained in the State Implementation Plan  (SIP) that the



Iowa Department of Environmental Quality (DEQ) submitted for lead



emissions is based on published emission factors.  The Iowa DEQ



determined estimated lead emissions from lead acid battery



plants differed significantly, depending on whether they were



based on emission factors or on actual test data.



     The purpose of this technical assistance effort by PEDCo



Environmental, Inc., for the EPA was to conduct a test program



that would provide the Iowa DEQ with lead and particulate emis-



sions data that can be used to determine whether the SIP for lead



emissions should be revised or the control strategies of lead



acid battery plants must be revised.
                               1-1

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     During the week of June 8,  1981,  PEDCo Environmental per-



sonnel conducted an emission sampling program at the Prestolite



lead acid battery plant in Manchester, Iowa, to determine lead



and particulate emissions at six process points selected by the



Iowa DEQ.
                               1-2

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                            SECTION 2

                         PROJECT SUMMARY



     Tables 2-1 and 2-2 present a summary of the emission data


collected at the six sampling locations during the testing

period.  A minimum of three lead tests and one particulate test

were conducted at each of the six emission points.  The purpose

of the long sampling time and the large volume of flue gas

sampled at each test site was to collect as large a sample as

possible to assure quality results.  Lead sampling and analytical

procedures followed those described in EPA proposed Method 12 of

the Federal Register.*  Particulate sampling and analytical

procedures followed those described in EPA Method 5 of the

Federal Register,** except that an ether-chloroform extraction

was performed on the impinger contents to determine condensible

organic and inorganic fractions.

     Table 2-3 presents the maximum and average yearly emission

data for total lead and particulate matter.  Emission data for

filterable and condensible (organic and inorganic) particulate

matter are also presented.  These values were calculated for the

six emission sources tested at the plant.  An example of the

calculations used to determine emission data on a yearly basis

is presented in Appendix A.  Both the yearly maximum and average

 *
  Federal Register, Vol. 45, No. 9, January 14, 1980.
**
  40 CFR 60, Appendix A, Reference Method 5, July 1, 1930.



                              2-1

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               TABLE  2-1.  SUMMARY OF  THE AVERAGE  LEAD AND PARTICULATE  EMISSION DATA
                              FOR THE  SIX SOURCES TESTED (METRIC UNITS)3
Source
Barton oxide
baghouse out-
let
Entoleter
scrubber out-
let
NJ
' Baghouse No. 1
*° outlet
Baghouse No. 2
outlet
Baghouse No. 3
outlet
Carter-Day
baghouse out-
let
Concentration, mg/dsm
Filterable
11.60


5.77



3.57

2.363

2.47

1.455


Particulate
Condensible
Organic
2.48


0.62



0.500

0.543

0.909

0.524


Inorganic
0.548


0.088



0.274

0.645

0.273

0.821


Total
14.63


6.478



4.344

3.551

3.652

2.80


Total
lead
6.65


0.887



1.56

0.525

0.729

0.163


Mass emission rate, kg/h
Filterable
0.06


0.10



0.16

0.11

0.13

0.07


Particulate
Condensible
Organic
0.01


0.01



0.02

0.02

0.05

0.03


Inorganic
o.or


0.00



0.01

0.03

0.01

0.04


Total
0.07


0.11



0.19

0.16

0.19

0.14


Total
lead
0.035


0.01



0.07

0.02

0.04

0.01


L
Percent lead
in total
particulate
45


15



40

15

20

5


Concentration 1n milligrams per dry standard cubic meter  (mg/dsm  )(20°C, 760 mm Hg), and mass emission rate in kilograms
 per hour (kg/h).

 Rounded to  the nearest 5 percent.

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                       TABLE 2-2.   SUMMARY  OF THE  AVERAGE LEAD  AND PARTICULATE EMISSION  DATA
                                      FOR THE SIX  SOURCES  TESTED  (ENGLISH UNITS)3
Source
Barton oxide
Entoleter
scrubber out-
let
Baghouse No. 1
outlet
Baghouse No. 2
outlet
Baghouse No. 3
outlet
Carter-Day
baghouse out-
let
Concentration, gr/dscf
Filterable
0.0054
0.0025


0.0013
0.0010
0.0011
0.0006
Particulate
Condensible
Organic
0.0011
0.0003


0.0002
0.0002
0.0004
0.0002
Inorganic
0.0002
0.0000


0.0001
0.0003
0.0001
0.0004
Total
0.0067
0.0028


0.0016
0.0015
0.0016
0.0012
Total
lead
0.0029
0.0004


0.0007
0.0002
0.0003
0.0001
Mass emission rate, Ib/h
Filterable
0.120
0.216


0.337
0.236
0.279
0.150
Particulate
Condensible
Organic
0.024
0.024


0.049
0.055
0.103
0.055
Inorganic
0.005
0.003


0.027
0.065
0.031
0.087
Total
0.154
0.243


0.413
0.356
0.413
0.292
Total
lead
O.U68
0.033


0.144
0.052
0.082
0.017
Percent lead
in total
particulate
45
15


40
15
20
5
to

U)
        Concentration in grains per dry standard cubic foot  (gr/dscf)(68°F,  29.92 in.Hg), and mass emission rate in pounds
        per hour (Ib/h).

        Rounded to the nearest 5 percent.

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                                    TABLE  2-3.   SOURCE  EMISSIONS  FROM PRESTOLITE  IN MANCHESTER,  IOWA
Source
Barton oxidec
Entoleter scrubber
Baghouse No. 1
Baghouse No. 2
Baghouse No. 3
Carter-Day bag-
house
Operating
schedule
h/day
24
16
16
8
8
8
days/yr
241
241
241
241
241
241
Total
Maximum emission rate, tons/yr
Filterable
1.31
0.86
0.83
0.32
0.35
0.20
3.87
Particulate
Condensible
Organic
0.21
0.05
0.09
0.05
0.10
0.05
0.55
Inorganic
0.04
0.01
0.05
0.06
0.03
0.08
0.27
Total
1.56
0.92
0.97
0.43
0.48
0.33
4.69
Total
lead
0.88
0.09
0.33
0.12
0.10
0.02
1.54
Average emission rate,*3 tons/yr
Filterable
1.08
0.42
0.65
0.23
0.27
0.14
2.79
Particulate
Condensible
Organic
0.21
0.05
0.09
0.05
0.10
0.05
0.55
Inorganic
0.04
0.01
0.05
0.06
0.03
0.08
0.27
Total
1.33
0.48
0.79
0.34
0.40
0.27
3.61
Total
lead
0.59
0.06
0.28
0.10
0.08
0.02
1.13
to
I
           Calculated from the sample run for each source that showed the highest emission rate.
           Calculated by averaging  the emission  rates for the sample runs at  each source.
          cBarton  oxide emissions represent both process lines and the secondary baghouse, based on the assumption  that emissions  from each stack
           are equal.

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emission rates for each emission point were based on the same


plant operating schedule.  The difference is that the maximum


emission rate was calculated using the highest individual sample


results, whereas the average emission rates represented the


average of all sample runs for each source tested.  Yearly


emission calculations were also based on the assumption that


plant operations will not change from what they were during the


testing period.  The yearly maximum and average total particu-


lates emitted by the plant are 4.69 tons/yr and 3.61 tons/yr.


Maximum and average total lead emissions are 1.54 tons/yr and


1.13 tons/yr.  All of these values are far below the total par-


ticulate and lead emission values determined for lead acid


battery plants by the use of emission factors.*


     Because the two Barton Oxide process lines and their control


devices are identical, lead and particulate emissions should be


similar, and they were considered equal for determining yearly


emissions.  Although emissions from the secondary baghouse


should be less, the emission rate calculated for the process


baghouse was used to determine yearly emissions for the secondary

baghouse.  For this reason the emissions reported in Table 2-3

are likely to be biased high.
*
 "Compilation of Air Pollution Emission Factors," (AP-42), Third
 Edition,  Prepared by EPA, August 1977.
                              2-5

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                            SECTION 3
                        PROCESS OPERATION

3.1  PROCESS DESCRIPTION
     The Prestolite lead acid battery plant produces both main-
tenance-free batteries (calcium lead alloy) and nonmaintenance-
free batteries (antimony lead alloy).  During the testing period
the plant had a normal operating output of about 3600 batteries
per day (bpd).  The maximum production output for the plant is
4100 bpd.   The methods used to produce the two types of batteries
are generally similar.  In those instances where the methods do
differ, each method used is discussed separately.  Figures 3-1
and 3-2 present process flow diagrams for the production of
antimony and calcium lead alloy batteries and indicate the
emission control devices used.
3.1.1  Grid Casting and Punching
     The first step in the production of an antimony battery is
the grid casting operation.  In the grid casting operation, an
automated process, molten lead is cast into two grids by machines,
The process was operated two shifts per day during the testing
period, and emissions are uncontrolled.
     Grids are produced for the calcium battery by a punching
process in which a continuous strip of lead attached to a spool
                               3-1

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                                                                       BARTON OXIDE
                                        GRID
                                       CASTING
                                  PASTING OPERATION
                                    POSITIVE AND
                                   NEGATIVE PLATES

BARTON
OXIDE
PROCESS

rxui-LiS B.n. nu. i
SECONDARY B.H.
BARTON OXIDE
PHOUSS B.H. NO.
ANTIMONY LEAD ALLOY
PASTE MIXING
POSITIVE AND NEGATIVE
PASTE
ENTOLETER
2
SCRUBBER
                                     PASTED PLATES
                                   OFF BEAR STATION
                                              PARTING OPERATION
                                                 AUTOMATIC
                                               PARTED  PLATES
                                              OFF BEAR STATION
TWO-STATIONS BAGHOUSE NO.2
                                              STACKING OPERATION
                                                AUTOMATIC
TWO-STATIONS BAGHOUSE NO.l
                                               STACKED ELEMENTS
                                                INSPECTION AND
                                               OFF BEAR STATION
                                              BURNING OPERATION
                                                    MAC
          BAGHOUSE NO. 3
                                                               BAGHOUSE NO.  2.
                                                 INSPECTION
                                                   STATION
                                                                   BATTERY REPAIR
   INTERCELL LINE NO. 1
      BAGHOUSE NO.  3
    INTERCELL  LINE NO.
    CARTER-DAY BAGHOUSE
BARTER-DAY
BAGHOUSE
ANTIMONY
BATTERY REPAIR
STATION


INSPECTION
STATION
          •EITHER «T OR DRY FORMATION IS USED.


Figure  3-1.    Process  flow  diagram  for the  production  of antimony
                              lead  alloy batteries.
                                          3-2

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                                                            BARTON OXIDE
ENTOLETER SCRUBBER

PASTING
OPERATION


CALCIUM LEAD
ALLOY PASTE MIX
ING OPERATION
ENTOLETER SCRUBBER ^


CARTER-DAY BAGHOUSE


^CARTER-DAY BAGHOUSE


CARTER-DAY BAGHOUSE


, CARTER-DAY BAGHOUSE



DRYING


CURING

PASTED
OFF
STA1


PLATES
SEAR
riON

ENTOLETER SCRUBBER t

DRY FORMATION
PROCESS
BREAK APART
STATION


WRAPPING
PROCESS
|
WRAPPED PLATES
INSPECTION
STATION


WRAPPED PLATES
OFF BEAR
STATION


BURNING
OPERATION
MAC



BAD WRAPPED
PLATES






CARTER-DAY BAGHOUSEj

^CARTER-DAY BAGHOUSE

INSPECTION
STATION


CALCIUM BATTERY
REPAIR STATION
CARTER-DAY BAGHOUSEr

BATTERY
ASSEMBLY



SHIPPING



ACID
CHARGE*

             •ONLY PERFORMED IF BATTERY WILL BE USED IN THE HEAR FUTURE.
Fiqure  3-2.  Process flow diagram for  the production of calcium
                         lead alloy batteries.
                                     3-3

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is fed into one of two punching machines.   The machine punches



the grid configuration into the strip of lead and feeds it to



another spool, which rewinds it.  This process was operated one



8-hour shift per day during the testing period, and emissions are




uncontrolled.



3.1.2  Barton Oxide Process



     The Barton Oxide Process is initiated by the addition of a



2050-lb hog to a hooded melting pot that is indirectly heated to



a temperature of 800°F.  When the hog melts, the molten lead is



evenly distributed between two separate Barton Oxide Process



lines by pouring the molten lead from the melting pot into each



of the two Barton Oxide reactor pots containing continuously



turning paddles.  The normal operating temperature of these




reactor pots  is between 720° and 750°F.  During the initial start-



up, gas burners are used to heat the reactor pots to the proper



temperature.  The gas burners are turned off when the proper



temperature is attained, and the temperature of each pot is



controlled by the amount of draft used.  Increasing the draft



across the pot decreases the pot temperature.



     As the lead is oxidized it gains weight by a factor of 1.04.



This means that a hog initially weighing 2050 Ib will weigh 2131



Ib when oxidized.



     Emissions from each reactor pot are controlled by separate



systems.  Each reactor pot is ducted through its own settling



tank, where larger particles drop out.  The off-gases are then




routed through two cyclones and a process fabric filter baghouse.



The effluents from each process baghouse are monitored




                               3-4

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by photoelectronics to detect excess emissions and corresponding



loss of material.  Should the baghouse experience a malfunction



that results in excess emissions, the system will automatically



shut down.  The particulate captured in the settling tank and two



cyclones is screw-conveyed to the bottom of the baghouse and



mixed with the particulate that is caught by the baghouse.  The



lead oxide (PbO) collected by the emission control system of each



Barton Oxide production line and that collected by the secondary



baghouse are mixed.  The mixture is then conveyed to an unmilled



tank and held there until it can be conveyed to a hammermill,



where it is beaten to the correct size.  From the hammermill, the



PbO is blown into Storage Tank C, where it is held for transfer



to either Storage Tank A or B.  From Tanks A and B, the paste



mixer operator draws the proper amount of PbO needed for the



paste mixing operation.  Any excess PbO is transferred to a



separate holding tank and sold to another Prestolite plant.



     Emissions from the melting pot, all the tanks, and those



conveyors that are maintained under a negative pressure are



controlled through sanitation ducts to a secondary baghouse.



     All Barton Oxide baghouses are on timers that periodically



turn them off to allow dust to settle.  This purging cleans the



system,  and reduces the pressure differential across the bag-



house.   Purging takes between 3 to 5 minutes.



     During the testing period both Barton Oxide process lines



operated 24 hours per day.
                               3-5

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3.1.3  Paste Mixing



     The plant operates three paste mixers.  Paste Mixers No. 1



and 2 are the Muller type and are identical; both produce paste



for antimony lead alloy batteries.  Paste Mixer No. 1 normally



makes paste used to produce negative plates, Paste Mixer No. 2



normally makes paste used to produce positive plates.  These two




mixers can produce either positive or negative paste as needed



and both operated two shifts per day during the testing period.



     The complete mix cycle time for either positive or negative



paste in Paste Mixers No. 1 and 2 is between 22 and 25 minutes



per batch.



     Mixing procedures for positive and negative paste are



similar.  Initially, PbO is charged into the mixer, which takes



approximately 1 minute.  Except for specialty paste, the amount



of PbO added to a batch is constant (2400 Ib).  After the PbO,



the fiber material and initial water are added.  Negative paste



uses about 14 to 15 percent more initial water than does positive



paste, but both pastes use the same amount of fiber material.



Production of negative paste also requires an expander agent,



which is added at this time.  The mixer is turned on during these



additions, and the batch time is recorded.



     After about 4 minutes of mixing the acid is added at a feed



rate of 1.5 to 2 gal per minute.  Positive paste uses about 12 to



13 percent more acid than does negative paste.




     The mixer continues to run until a predetermined peak tem-



perature is reached, about 150°F.  At this point the cooling






                                3-6

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system is turned on until the paste being mixed reaches a tem-



perature of 110°F.  At this point the mixer is turned off to



allow the test booth to determine the density and hardness of the



paste mix.  The paste is tested just before it is needed by the




pasting operation.



     The first test run on the mixed paste is to determine its



cube weight (density).  If the cube weight of the paste is low,



PbO is added and it is remixed for 2 to 3 minutes.  If the cube



weight is high, either water or acid is added separately or in



combination and the paste is remixed for 2 to 3 minutes.



     The second test run is a penetration (hardness) test.  If



the penetration test shows that the paste is too soft, acid is



added to the mix; if the paste is too hard, water is added.  If



either addition is made the paste is remixed for 2 to 3 minutes.



     After the paste has been remixed it is retested.  If the



paste still does not meet the specifications, corrective addi-



tions are made until the paste is acceptable.  When the paste is



acceptable, it is dumped through a door in the bottom of the



mixer into the pasting chute, which directs it to the pasting



machine.



     The third paste mixer produces paste for calcium lead alloy



batteries.  This mixer operated during the first shift throughout



the testing period,  except on the first day (when it was not



operating at all).  The mixing procedure for calcium lead alloy



paste is similar to that of the two antimony lead alloy paste



mixers.   The PbO, initial water, fiber material, and acid additions





                              3-7

-------
for calcium lead alloy paste are very close to the amounts used



to make negative antimony lead alloy paste.  The primary dif-



ferences are that the mix time for calcium paste is about 40



minutes, and the paste requires twice as much expander  (of a




different type).



     The emissions from all three paste mixing machines and the



test booth are controlled by an Entoleter scrubber.



3.1.4  Plate Pasting



     Two identical antimony lead alloy battery plate pasting



machines operated two shifts per day during the testing period.



One machine normally pastes negative plates and receives all its



paste from Paste Mixer No. 1; the other machine normally pastes



positive plates and receives all its paste from Paste Mixer No. 2,



     At the beginning of the pasting operation on each machine,



the operator removes the connected grids from skids and loads



them into the machine.  The grids are then automatically fed



through the machine, where the paste is applied to them.  The



operator feeds paste from a chute into the pasting machine to



maintain the amount of paste at a proper level.  After  the paste



has been applied to the plates, a connected closed system con-



veys them through the drying and curing operations to the off-



bear station, where an operator inspects them and removes the



bad ones.  The operator then stacks the good plates together and



brushes any loose paste off of the top of them before putting



them on skids to be sent either to the dry formation process or



directly to the parting operation.
                               3-8

-------
     Emissions from the paste application, drying, and curing



operations are not controlled.  Emissions from the off-bear



station are controlled by Baghouse No. 1.



     The plant has one plate pasting machine for calcium lead



alloy batteries, which operated one shift per day during all but



the first day of the testing period.  This machine receives all



its paste from the calcium lead alloy paste mixer.  Mixed paste



for the calcium lead alloy pasting machine is dumped into a



hopper located above the mixer.  An operator feeds the paste into



the pasting machine as needed.



     The pasting operation for calcium lead alloy batteries is



different from that of the other two pasting machines.  In this



operation the operator loads a spool of grid material into the



pasting machine, which is automatically fed, and the grid mate-



rial is pasted.  After the paste has been applied to the grid



material and the plates have been cut to the proper size, a con-



nected closed system conveys them through the drying and curing



operations to the off-bear station, where an operator performs



the same operations as those performed at the antimony lead alloy



battery plate stations.  When they leave the off-bear station,



the calcium lead alloy plates are sent to the wrapping operation.



     The pasting and off-bear operations are hooded and ducted to



the Entoleter scrubber.  Emissions from the cutting, drying, and



curing operations are not controlled.
                               3-9

-------
3.1.5  Parting Operation




     Some parting of antimony lead alloy plates is done auto-



matically and some is done manually.  The automatic plate part-



ing machines operated one shift per day, while the manual plate



parting operation varied between one and two shifts per day



during the testing period.  In both methods the operators re-



ceive either dry formation or hydroset unparted plates, depend-



ing on whether they are to be used in a dry or wet battery.



     Two automatic parting machines were operating during the



testing period.  At each machine an operator loads the unparted



plates into the machine, which separates (parts), brushes, and



clips the lugs.  The lugs are clipped so that they will fit in



the MAC machines.



     The parted plates are conveyed to an off-bear station,



where an operator removes them and puts them into a tub to be



sent to the stacking operation.



     Emissions from both the parting machines and the off-bear



stations are controlled by Baghouse No. 1.



     A manual or band saw operation is used when the lugs do not



have to be brushed or clipped.  In this process the operator



first removes a handfull of either dry-formed or hydroset



plates from a skid and then aligns the plates so that the band



saw will separate the two plates evenly.  After the plates are



sawed, the operator puts the separated plates in a tub to be sent




to the stacking operation.  Emissions from the sawing operation



are controlled by Baghouse No. 1.




                                3-10

-------
3.1.6  Stacking Operation



     Stacking of antimony lead alloy plates is done both auto-



matically and manually; both operated two shifts per day during




the testing period.



     At each of the two automated stacking machines an operator



loads positive plates, negative plates, and separators into the



machine.  The machines automatically stack alternating negative



plate, separator, and positive plate until the desired element



size has been assembled.



     After they are stacked, the elements are conveyed to an off-



bear station, where an operator first verifies that the correct



amount of plates have been stacked to form the element and then



places them onto a skid.  The elements are then sent to the MAC



or Tiegel departments for the burning operation.  Emissions from



the two automated stacking machines and two off-bear stations are



controlled by Baghouse No. 1.



     At each of the four hand-stacking stations an operator piles



three separate stacks, one of positive plates, one of negative



plates, and one of separators.  The operator then stacks the



plates by alternating between negative, separator, and positive



plates until the proper size element is assembled.  If the ele-



ments are to be sent to the antimony lead alloy MAC burning



operation, the top of the element is first dipped in a flux,



which increases the bond strength of the casted strap.  If the



elements are to be sent to the Tiegel burning operation, they are



not fluxed.
                              3-11

-------
     Emissions from two of the hand stacking stations are con-




trolled by Baghouse No. 1; emissions from the other two are



controlled by Baghouse No. 2.



3.1.7  Wrapping



     Two wrapping process lines for calcium lead alloy batteries



were operated for one shift per day during the testing period.



     The first station in the wrapping process is the break-



apart station, which is a manual operation.  An operator sepa-



rates and sorts the positive plates to be wrapped.  The operator



also applies a flux to the top of the positive plates, which aids



in the fusion of the plates at the MAC cast-on process.  From the



break-apart station the positive plates go to the wrapping



machine, where the operator inserts the positive plates into the



machine, which automatically wraps all but the top of the plate



in a rubber-like substance.  From the wrapping machine the



positive plates are conveyed to an inspection station, where the



wrapping material is inspected for holes, mis-cuts, etc.  The



inspector removes badly wrapped plates and sends them back to the



break-apart station, where they are unwrapped and then sent back



through the wrapping machine.



     At the inspection station the operator places a negative



plate on top of the wrapped positive plate.  The plate is then



conveyed from the inspection station to the off-bear station,



where an operator groups the positive and negative plates into




the required element size and places them on a skid.  The skids
                               3-12

-------
are sent either to storage or to the four calcium lead alloy



battery MAC machines as needed.



3.1.8  Burning Operation



     Two separate departments contain MAC machines, and both



operated one shift per day during the testing period.  One



department performs the burning operation for calcium lead alloy



batteries only, and the other performs the burning operation for



antimony lead alloy batteries only.



     During the testing period only three of the four calcium



lead alloy MAC machines operated.  At each MAC machine the



operator receives the elements on a skid and stages those that



will be used in the battery.  All the elements are placed in a



slotted holder that separates them by the proper distance from



each other.  When all the elements are in the holder they are



aligned by a machine and clamped into place.



     While this is taking place the mold is being heated, and



when it reaches a preset temperature, the element holder will



automatically rotate (turn upside down) so that the top of the



elements are just above the mold.  The mold is then filled with



molten lead, the elements are lowered into the mold, and the



positive and negative plates are connected with separate cast-on



straps.  At this time the operator applies glue to the bottom of



the elements.  When the mold reaches a preset cooling temperature,



the elements and connecting cast-on straps are released from the




mold and the holder reverts back to an upright position.  The
                                3-13

-------
operator releases the elements from the holders and removes the



casted element, which is placed into a battery case.



     The battery is then placed on a conveyor line that goes to



one of two inspection stations:  one for automobile batteries



and the other for heavy-duty batteries.



     The molten lead used in the MAC machines comes from a lead



pet.  Each lead pot supplies molten lead to two MAC machines.



The melting pot is charged with lead ingots, which it melts down



electrically at a temperature of about 800°F.  The ingots are



normally charged in groups of three.  To furnish molten lead to



each MAC machine operating one shift per day requires the melt-



ing of about 10 ingots.



     At the MAC automobile battery inspection station each



battery cell is probe-checked for continuity shorts.  All ac-



ceptable batteries are conveyed to the through-the-partition



(TTP) machine, which is an intercell welding operation and the



first step in the battery assembly process.



     All rejected batteries are sent to the calcium lead alloy



battery repair station, where the problem is analyzed.  If the



problem is a bad wrap, the wrap is replaced and the battery is



sent to the TTP machine.  If a plate is defective, it is scrapped



and the other plates are sent back to the MAC machine to be



reworked.



     The plant has one heavy-duty battery intercell and inspec-



tion station, which is operated in the same manner as the auto-



mobile battery inspection station.  After inspecting the battery
                                3-14

-------
the operator intercell burns each individual cell in the battery



and checks it by reprobing.  Good batteries are put onto a skid



and sent to a storage area.



     The emissions from the four MAC machines, two melting pots,



and one repair station for calcium lead alloy batteries are



controlled by the Carter-Day baghouse.  Emissions from the TTP



machine and two inspection stations are uncontrolled.



     The plant has seven antimony lead alloy MAC machines, which



are operated in basically the same manner as the calcium lead



alloy MAC machines except for the method of putting the casted



element into the battery case.  These MAC machines have an option



that allows the cast element of certain types of batteries to be



placed into the battery case automatically.



     The cast elements from all the antimony lead alloy MAC



machines are sent to one inspection station, where the operator



checks the continuity of each element and removes any excess



material.  The operator puts all good batteries on one skid,



which is sent to the battery assembly area.  All rejected bat-



teries are put on another skid, which goes to a battery repair



station.



     Emissions from the antimony lead alloy MAC machines are



controlled by Baghouse No. 2.  Emissions from the inspection



station are uncontrolled.  Emissions from the antimony lead alloy



battery repair station, which operated one shift per day during




the testing period, are controlled by the Carter-Day baghouse.
                              3-15

-------
     The plant has 10 Tiegel machines, which are divided into two



production lines that operated one shift per day during the test-



ing period.  The Tiegel machines perform the burning operation



for antimony lead alloy batteries only.  The operator at each



machine receives hand- and machine-stacked elements on skids from



the stacking area.  After placing the proper amount of elements



needed to produce a battery into a mold in the Tiegel machine,



the operator then places two posts into the elements, one for the



negative plates and one for the positive plates.  The purpose of



the molds is to hold and space the number of elements needed to



form a battery.  After the proper number of elements have been



placed into the mold, the operator manually melts two straps, one



to connect the positive plates and its post and one to connect



the negative plates and its post.



     After the straps are connected to the plates, the operator



releases the elements from the mold and places the burned ele-



ments onto a table.



     Another operator, called a "sinker," is located on the other



side of the table.  This operator turns over the burned elements,



puts glue on the bottom of them, and places them into a battery



case.



     The cased battery is then sent to the intercell burning



operation, which operated one shift per day during the testing



period.  There is one intercell burning operation for each Tiegel



machine production line.  The operator of the intercell burning



operation burns a connector onto each element to connect the






                              3-16

-------
positive and negative plates.  The batteries are then inspected

for continuity, and good batteries are sent to the battery

assembly area, rejected batteries are sent to the antimony lead

alloy repair station.

     Emissions from the 10 Tiegel machines and Intercell Station

No. 1 are controlled by Baghouse No. 3.  Emissions from Intercell

Station No. 2 are controlled by the Carter-Day baghouse.  Emis-

sions from the two battery inspection stations are uncontrolled.


3.2  ENVIRONMENTAL CONTROL DEVICES TESTED

     The emissions from six different control devices were sam-

pled during the testing period.  The following is a list of the

these devices and the process emissions they control.

     1.   Barton Oxide Process Baghouses

          a)   Barton Oxide Process Line 1.

          b)   Barton Oxide Process Line 2.

     2.   Entoleter Scrubber

          a)   Two antimony lead alloy battery paste mixers.

          b)   The calcium lead alloy battery paste mixer.

          c)   The paste mixer quality test booth.

          d)   Calcium lead alloy pasting machine.

          e)   Calcium lead alloy pasting operation off-bear
               station.

     3.   Carter-Day Baghouse

          a)   Three wrapping process lines, including the break-
               apart station, wrapping machine, inspection sta-
               tion, and off-bear station for each.

          b)   Four calcium lead alloy battery MAC machines.
                               3-17

-------
          c)    Two calcium lead alloy battery MAC melting pots.

          d)    The calcium lead alloy battery repair station.

          e)    The antimony lead alloy battery repair station.

          f)    Tiegel Intercell Line'No.  2.

     4.    Baghouse No.  1

          a)    Two hand-stacking stations.

          b)    Two automatic stacking machines.

          c)    Two off-bear stations, one for each automatic
               stacking machine.

          d)    Two off-bear stations, one for each antimony lead
               alloy battery pasting line.

          e)    Three automatic parting machines.

          f)    Three parted-plate off-bear stations, one for each
               automatic parting machine.

          g)    One manually operated parting machine.

     5.    Baghouse No.  2.

          a)    Two hand-stacking stations.

          b)    Seven antimony alloy battery MAC machines.

     6.    Baghouse No.  3.

          a)    Ten Tiegel machines.

          b)    Tiegel Intercell Line No.  1.


3.3  PROCESS DATA

     Production data for each process are presented in the fol-

lowing sections.  These data are grouped according to the device

used to control emissions from each specific process.  When con-

trol devices regulated emissions from more than one process, the

production data are presented separately for each specific
                               3-18

-------
process.  For certain processes, the production data reported



represent an average of the total amount produced during the



shift or shifts operating during the sampling period because



that it is the only method used by the plant to record produc-



tion.  All production data presented were recorded by plant



personnel.  The plant determines the production rate for most



processes by calculating an equivalent number of batteries



produced by the process.  For purposes of this calculation,



a contingency factor has been determined for each process that



takes into account production losses, including rejected com-



ponents.  The equivalent number of batteries produced for each



process is calculated by dividing the production rate by the



contingency factor for that process.  Example calculations are



contained in Appendix A.



3.3.1  Barton Oxide Process Baghouses



     The amount of PbO produced by the Barton Oxide process is



determined from the number of hogs charged during the sampling



period.  The number of hogs charged was divided by two because



only half of the melted lead goes to each Barton Oxide process



line.  The number of hogs charged during the first and second



shifts of each testing day was determined from the plant produc-



tion logs, and this value was used to calculate the average



number of hogs melted during the sampling period.  Table 3-1



presents the production data for the Barton Oxide process lines



during the sampling periods.
                              3-19

-------
                       TABLE 3-1 .  PROCESS INFORMATION AND CALCULATED PRODUCTION RATES FOR THE
                                 BARTON OXIDE PROCESS TESTED DURING EACH SAMPLE
Date
(1981)
6/8
6/8
6/9
6/9
Run.
No.b
2BOL-1
2BOL-2
2BOL-3
1BOP-1
Length of
test, h
4.0
2.0
2.0
2.0
Number
of hogs
charged
6.0
3.0
3.4
3.4
Amount of
PbO produced
per line, 1b
6,400
3,200
3,600
3,600
Average
draft,0
(in. H20)
0.58
0.55
0.66
0.56
Average
melting pot
temperature,
°F
800
795
795
795
Barton oxide
reactor inside
temperature,
°F
730
740
730
725
Production
rate of
PbO,
Ib/h
1,600
1,600
1,800
1,800
u>
I
NJ
O
       All plant readings were recorded at a specific time and not integrated over a time period.  The values
     "^reported above represent an average of these instantaneous values over an entire sample run.

       All lead tests were performed on emissions from Barton Oxide Process Line 2; the particulate test
       (1BOP-1) was performed on emissions from Barton Oxide Process Line 1.

      °Static pressure drop.

-------
     Each hog charged to the Barton Oxide melting pot weighs




about 2050 Ibs; when it is oxidized to PbO, the weight increases



by a factor of 1.04.  Calculations of all production data are



based on the assumption that all of the melted lead is oxidized



to PbO.  The production rate of PbO averaged 1700 Ib/h for each



Barton Oxide process line during the testing period.



3.3.2  Entoleter Scrubber



     Production data for the paste mixing operation are based on



the number of batches of paste mixed during each sample run,



which were determined from the plant's production log.  Table



3-2 presents the production data for the paste mixing operation.



     The calcium lead alloy pasting machine and off-bear station



production data are combined because each plate that is pasted is



handled at the off-bear station, even if it is rejected.  Table



3-3 presents the production data for these two operations during



the testing period.  The production data are determined on a per-



shift basis.  The number of plates pasted and handled at the



off-bear station is directly proportional to the number of



batches of paste mixed.  Because the number of batches of paste



mixed during each test is known, a calculation can be made to



determine the number of plates pasted and handled at the off-



bear station during each sample run.  The same type of plate was



being pasted throughout the testing period.  The average equiva-



lent number of batteries produced at the calcium lead alloy



pasting and off-bear station during the testing period was 139



batteries per hour.





                                3-21

-------
                                TABLE 3-2.   CALCULATED  PASTE  MIXING PRODUCTION DATA DURING EACH RUN
to
to

Date
(1981)
6/8





6/9



6/10



Run
No.
ESL-1





ESL-2C
ESP-1


ESL-3


Batch number and time mixing cycle commenced
Antimony lead alloy paste mixers
Mixer No. 1 (negative paste)
Batch No.
4
5
6



3
4
5

3
4
5
Time, h
10:47
14:14
21:01



8:20
9:25
10:27

7:41
9:02
10:20
Mixer No. 2 (positive paste)
Batch No.
4
SK
6£
7b
8b
9
3
4
5

2
3
4
Time, h
10:55
14:08
15:30
16:50
18:55
20:58
8:16
9:20
10:34

8:21
9:08
9:56
Calcium lead alloy
paste mixer
Batch No.
a





3
4
5
6
3
4
5
Time
a





8:30
9:09
9:49
10:39
8:20
9:10
9:53
Production
rate,
batches
per hour
3.1





4.0



3.3


                   'Process did not operate on this date.

                    Negative paste was mixed in these batches.

                   cESL-2 and ESP-1 sample runs were performed simultaneously.

-------
                           TABLE  3-3.   CALCULATED CALCIUM LEAD ALLOY PRODUCTION DATA FOR THE PASTING
                                          AND  OFF-BEAR STATIONS DURING EACH SAMPLE RUN
Date
(1981)
6/8
6/9
6/10
Run
No.
ESL-13
ESL-2b
ESP-1
ESL-3
Total
length of
test, min
176
144
163
Number of plates
pasted and handled
at off-bear station

39,883
32,364
Equivalent
number of
plates per
battery

103
103
Batteries produced
Equivalent
number

387
314
Equivalent
number
per hour

161
116
U)
I
N)
U>
      Process  did not operate on  this  date.

     DRuns ESL-2 and ESP-1  were conducted simultaneously.

-------
3.3.3  Baghouse No. 1



     Production data for each of the two separate antimony lead



alloy off-bear stations are dependent on the number of plates



pasted at each pasting line because every plate pasted is con-



veyed to its off-bear station.  The plant determines the pro-



duction data for the two off-bear stations on a per-shift basis.



Table 3-4 presents the production data for the two off-bear



stations during the testing period.  The average equivalent



number of batteries produced at the two antimony lead alloy off-



bear stations during the testing period was 231 batteries per



hour.




     Production data for the two automated parting machines that



operated during the testing period and their respective off-bear



stations are combined because each parted plate is handled at an



off-bear station.  Table 3-5 presents the production data for the



automated parting machines and off-bear stations during the



testing period and also for the manually operated parting machine.



The average equivalent number of batteries produced from both the



automatic and manual parting machines during the testing period



was 335 batteries per hour.



     Production data for the two automatic stacking machines and



their respective off-bear stations are combined because after the



plates are stacked they are conveyed to a off-bear station.



Table  3-6 presents the production data for the automatic stacking




machines and off-bear stations during the testing period.  This



table also includes the production data for Hand-Stacking Stations






                                3-24

-------
                          TABLE 3-4.   CALCULATED PRODUCTION  DATA FOR  THE TWO  ANTIMONY LEAD  ALLOY
                                           OFF-BEAR STATIONS DURING EACH SAMPLE RUN
Date
(1981)
6/10
6/10
6/10
6/11
Run
No.
B1L-1
BIL-Z8
B1P-1
B1L-3
Total
length of
test, win
196
196
196
168
Number of pasted
plates handled at
off-bear station
From pasting
Line 1
32,383
30,738
30,611
20,852
From pasting
Line 2
24,908
23,273
23,147
31 ,409
Total number
of plates
handled at
off-bear station
57,291
54,011
53,758
52,261
Equivalent
plates per
battery
75
75
75
75
Batteries produced
Equivalent
number
764
720
717
697
Equivalent
number
per hour
234
220
219
249
                     "Sampling times for Run Nos. B1L-2 and B1P-1 overlapped.
N)
Ul
TABLE  3-5.  CALCULATED PLATE  PARTING  PRODUCTION DATA
                 DURING  EACH SAMPLE RUN



Date
(1981)
6/10
6/10

6/10
6/11



Run
No.
B1L-1
B1L-28

B1P-1
B1L-3


Total
length of
test, min
196
196

196
168
Number of parted plates
handled at off-bear station
From automatic
parting machine
No. 1
30,581
6,241*

I,369C
26,079
No. 2
16,730
From manual
parting machine
station
32,224
3,414^ 31,831
I
2,390'
24,480
31 ,801
14,905

Total number of
parted plates
handled at off-
bear stations
79,535
41,486

38,560
65,464

Equivalent
number of
plates per
battery
72
72

72
72

Batteries produced

Equivalent
number
1,105
1,105

1,105
909
Equivalent
number
per hour
338
338

338
325
                    "Sampling  times for Run Nos.  B1L-2 and B1P-1  overlapped.
                     Process operated during only 20 percent of the sample  run.
                    cProcess operated during only 15 percent of the sample  run.

-------
              TABLE  3-6.  CALCULATED ELEMENT STACKING PRODUCTION DATA  DURING  EACH SAMPLE  RUN
u>
I
to
(Ti
Date
(1981)
6/10
6/10
6/10
6/11
Run
No.
B1L-1
B1L-28
B1P-1
B1L-3
Total
length of
test, mln
196
196
196
168
Number of stacked elements
bandied at off -bear station
From au
stacking
No. 1
1,722
787
715
576
tomatlc
machine
No. 2
722
750
752
640
From
stacklnq
No. 3
752
516
390
440
hand-
machine
No. 4
717
588
578
359
Total number
of stacked
el ements
handled
3,913
2,641
2,435
2,015
Equivalent
number of
elements per
battery
5.4
5.4
5.4
5.4
Batteries produced
Equivalent
number
728
491
453
375
Equivalent
number
per hour
223
150
139
134
             "Sampling times for Run Nos. B1L-2 and B1P-1 overlapped.

-------
No. 3 and 4.  The equivalent number of batteries produced by the



stacking stations during the testing period was 162 batteries per




hour.



     The plant records the production data for these operations



on a per-shift basis.  For calculation of the number of plates



parted or stacked during the testing period it was assumed that



the daily production rate was constant in that testing occurred




during normal process operating conditions.  The production dur-



ing each sample run was calculated by dividing the total sample



time by the actual operating time during a shift and then multi-



plying by the average production rate for the shift.  Large



variations in production rates for the automatic and hand stack-



ing operations can be attributed to the type of element being



stacked during the testing period.



3.3.4  Baghouse No. 2



     Production data for Hand-Stacking Stations No. 1 and 2 are



recorded by the plant once per shift.  For calculation of the



number of elements stacked during the testing period, it was



assumed that the daily production rate was constant in that



testing was performed during normal process operating conditions.



The production during each sample run was calculated by dividing



the total sampling time by the actual operating time during an



entire shift and then multiplying by the average production rate



for the shift.  Table 3-7 presents the production data for the



Hand-Stacking Stations No. 1 and 2 during the testing period.  The
                              3-27

-------
                    TABLE  3-7.  CALCULATED ELEMENT STACKING PRODUCTION DATA  DURING  EACH SAMPLE RUN
10
 I
K)
00
Date
(1981)
6/11
6/11
6/12
6/12
Run
No.
B2L-1
B2L-2
B2L-3*
B2P-1
Total
length of
test, m1n
168
168
168
168
Number of stacked elements
handled at off-bear station
From hand-stackinq stations
No. 1
405
405
455
455
No. 2
345
345
421
421
Total number
of stacked
elements
handled
750
750
876
876
Equivalent
number of
elements per
battery
5.4
5.4
5.4
5.4
Batteries produced
Equivalent
number
140
140
163
163
Equivalent
number
per hour
50
50
58
58
                  aThe sampling times for Run Nos. B2L-3 and B2P-1 overlapped.

-------
average equivalent number of batteries produced at these stations



during the testing period was 54 batteries per hour.



     Production data for the seven antimony lead alloy element-



burning MAC machines are recorded by plant personnel on an hourly



basis.  The number of batteries burned during a sample run was




calculated by performing a summation of the hourly production



rates during the sampling period.  For sample runs in which the



testing times overlapped into a portion of an hour, the fraction



of the hour sampled was multiplied by the hourly production rate.



The average number of batteries burned during the testing period



was 159 batteries per hour.  Table 3-8 presents the production



data for the seven antimony lead alloy MAC machines during the



testing period.



3.3.5  Baghouse No. 3



     Production data for the 10 antimony lead alloy Tiegel



machines and Tiegel Intercell Line No. 1 are recorded by plant



personnel on a hourly basis.  The number of batteries burned and



intercells connected during a sample run was calculated by



summing the hourly production rates during the sampling period.



When the testing time overlapped into a portion of an hour, the



fraction of the hour sampled was multiplied by the hourly pro-



duction rate.  The average number of batteries burned by the 10



Tiegel machines was 103 batteries per hour.  Table 3-9 presents



the production data for these operations during the testing



period.
                              3-29

-------
 I
u>
o
                           (TABLE  3-8.  CALCULATED PRODUCTION  DATA FOR THE  ANTIMONY  LEAD ALLOY
                                              MAC  MACHINES  DURING EACH SAMPLE RUN
Dtte
(1981)
6/11
6/11
6/12
6/12
Run
No.
B2L-1
B2L-2
B2L-3b
B2P-1
Total length
of sample
run, m1n
168
168
168
168
Number of batteries burned by the seven MAC machines
No. 1
168
40
a
a
No. 2
a
7
95
93
No. 3
57
a
a
a
No. 4
132
135
116
112
No. 5
a
a
a
a
No. 6
164
137
a
a
No. 8
151
142
141
137
Total
batteries
burned
620
461
352
342
Batteries
burned
per hour
221
165
126
122
                'Process did not operate during the sampling period.
                ''The sampling times for Run Nos. B2L-3 and B2P-1 overlapped.
                               TABLE 3-9.  CALCULATED PRODUCTION DATA  FOR THE ANTIMONY
                         BATTERY TIEGEL MACHINES AND INTERCELL LINE 1  DURING EACH  SAMPLE RUN
fete
(1981)
6/9
6/10
6/10
6/11
6/11
Run
No.
B3L-1
B3L-2
B3L-3
B3L-4
B3P-1
Total length
of test, m1n
68
196
154
154
149
Number of batteries burned by the ten Tlegel machines
Tleael machine
No. 1
18
59
50
57
53
No. 2
14
53
38
40
34
No. 3
18
168
142
63
56
NO. 4
17
73
47
63
48
No. 5
17
49
37
44
30
No. 6
11
110
51
76
48
No. 7
17
64
42
51
47
No. 8
41
138
76
109
62
No. 9
11
97
54
52
36
No. 10
13
66
50
50
41
Total
burned
177
877
587
605
455
Number
burned
per hour
156
268
229
236
183
Batteries frow
Intercell Line 1
Total
burned
84
402
314
267
221
Number
burned
per hour
74
123
122
104
90

-------
3.3.6  Carter-Day Baghouse



     Production data for the No. 1 and 2 wrapping process lines



which operated during the testing period were recorded by plant



personnel at the beginning and end of each sample run.  The



production data reported on Table 3-10 represent the total number



of plates wrapped during each sampling period.  During the test-



ing period an average of 4262 plates were wrapped per hour.



     Production data for the Tiegel Intercell Line No. 2 were re-



corded by plant personnel on a hourly basis.  During the testing



period an average of 122 batteries per hour were burned on the



intercell line.  Production data for the Tiegel Intercell Line



No. 2 during the testing period are also included in Table 3-10.



     Production data are grouped together for the calcium lead



alloy MAC Machines No. 1, 3, and 4; automobile battery inspection



station; and the heavy-duty battery inspection, and intercell



station that operated during the testing period because all



calcium lead alloy batteries burned at these three MAC machines



are sent either to the automobile or to the heavy-duty battery



inspection stations.  During the testing period, production data



for these processes were recorded by plant personnel at the



beginning and end of each sample run.  Table 3-11 presents these



data.  An average of 104 batteries per hour were burned during



the test period.



     The number of lead ingots melted at the two calcium lead




alloy melting pots is not recorded, but it is dependent on the




number of elements burned at the MAC machines.





                               3-31

-------
                       TABLE  3-10.  CALCULATED PRODUCTION DATA FOR THE  WRAPPING  PROCESS  AND
                                        INTERCELL LINE  2 DURING  EACH SAMPLE RUN
Date
(1981)
6/8
6/8
6/10
6/11
Run
No.
CDL-1"
CDP-1
COL-Z
COL- 3
Total length
of test, m1n
251
252
251
252
Number of plates wrapped
Wrapping line
No. 1
6,831
6,831
8,338
10.432
No. 2
9.694
9.694
8,130
11.591
Total plates
wrapped
16,525
16,525
16,468
22,023
Number wrapped
per hour
3,934
3,934
3,937
5,244
Batteries from Intercell Line 2
Total
burned
430
430
625
565
Number burned
per hour
102
102
150
135
                  *Run Nos. CDL-1 and COP-1 were sampled simultaneously.
U)
U)
to
TABLE  3-11.   PRODUCTION DATA  FOR THE  CALCIUM BATTERY MAC  MACHINES  AND
           INSPECTION STATIONS CALCULATED DURING  EACH SAMPLE RUN
Date
(1981)
6/8
6/8
6/10
6/11
Run
No.
COL-1*
CDP-1
CDL-2
CDL-3
Total
length of
test, mln
251
252
251
252
Number of calcium lead alloy batteries burned
1
No. 1
193
193
160
174
No. 2
a
a
a
a
we
No. 3
173
173
134
180
No. 4
121
121
a
127
Total
burned
487
487
294
481
Number burned
per hour
116
116
70
115
Automatlve batteries
Total
Inspected
366
366
294
354
Number Inspected
per hour
87
87
70
84
Heavy-duty and
Intercell connected
batteries
Total
Inspected
121
121
a
127
Number Inspected
per hour
29
29
a
30
            *Run Nos. COt-1 and COP-1 were sampled simultaneously.

-------
     The plant does not record any production data for the two



separate antimony and calcium lead alloy battery repair stations,



but plant personnel indicated that between 150 and 180 elements



are repaired at each station during a normal shift.
                              3-33

-------

-------
                            SECTION 4



                SAMPLE LOCATIONS AND TEST METHODS






     The following sections describe the sampling sites and out-



line the test methods that were used to determine emissions of



total lead, filterable particulate matter, and condensible



(organic and inorganic) particulate matter.






4.1  BARTON OXIDE PROCESS BAGHOUSES NO. 1 AND NO. 2



     Total lead and filterable particulate emissions were mea-



sured at the outlet of the Barton Oxide Process Baghouse No. 2,



as shown in Figure 4-1.  Filterable and condensible particulate



emissions were measured at the outlet of Baghouse No. 1.  Both



baghouses and sampling locations are identical.  On both stacks



two sample ports, 90 degrees apart, were located 13.8 duct diam-



eters downstream and 12 duct diameters upstream from the nearest



flow disturbances in the 13.5-inch I.D. round stacks.  Eight



sampling points, four per port, were used to tranverse the



cross-sectional area of a given stack during a test run.



     The 30-minute sampling time at each point for the first lead



test yielded a total test time of 240 minutes.  The sampling time



for the other two lead tests and one particulate test was reduced




to 15 minutes per point, which yielded a total test time of 120




minutes.  Sampling times were reduced because of the heavy grain



loading found on the filter of the first lead test.





                              4-1

-------
                  ROOF
                  EDGE
                                            TRAVERSE POINT
                                                  NO.
                                                  1
                                                  2
                                                  3
                                                  4
                           DISTANCE,
                              in.
                             1.0
                             3.4
                            10.1
                            12.5
DUCT I.D.  = 13.5 in.
PORT I.D.  = 3 in.
NIPPLE LENGTH = 3.5 in.
                    13.5 in.  13.5 in.  13.5 in.
                      I.D.     I.D.     I.D.
1
UPS'
i
'REAM
13.5 ft
12 duct
diameters
(dd
i
i

)
i


DOWNSTREAM
15.5 ft
13.8


dd
f









\
\
FLOW
L











X









t
\
FLOW
n











yJ




/



\
\
FLOW
S




.-PORT CENTER-LINE
/_
3.0 ft UPPER ROOF LEVEL
t





                   SECONDARY PROCESS  PROCESS
                   BAGHOUSE    LINE    |_INE NO.
                             NO. 1
                            BAGHOUSE
BAGHOUSE
                    LOWER ROOF LEVEL
      Figure  4-1.   Barton oxide process and secondary baghouse outlet.
                                    4-2

-------
4.2  ENTOLETER SCRUBBER OUTLET
     Total lead, filterable particulate, and condensible (organic
and inorganic) particulate emissions were measured at the outlet
of the Entoleter scrubber, as shown in Figure 4-2.  Two sample
ports, 90 degrees apart, were located 2.2 duct diameters upstream
and 7.5 duct diameters downstream from the nearest flow distur-
bances in the 25-inch I.D. round stack.  Sixteen traverse points,
eight per port, were used to traverse the cross-sectional area of
the stack during each test run.
     Because the length of each sample run depended on the opera-
tion of the paste mixers, variations occurred in the test times.
The sampling times for the three lead tests were 176, 144, and
163 minutes.  The sampling time for the particulate test, which
was run simultaneously with the second lead test, was 144 min-
utes.  If the initial estimate for the length of a sample run was
insufficient because of a variation in the paste mixing opera-
tion, the sampling time was increased.  The reason for increasing
the sample time was to assure that the sample run would be con-
ducted during the entire mixing cycle so as to not bias the re-
sults.  This was done by estimating the amount of time left in
the paste mixing operation and dividing it into equal segments to
allow each sample point on a single traverse to be sampled for
the same amount of time.  Sampling was done on only one traverse
for the extra time period because changing ports would involve
too much time.
     The initial lead test was run for 11 minutes per point.  The
other two lead tests and one particulate test were initially run
                              4-3

-------
                                       TRAVERSE POINT
                                             NO.
  DUCT  I.D.  =  25  in.
  PORT  I.D.  =  3  in.
  NIPPLE  LENGTH  =3.5  in.
             1
             2
             3
             4
             5
             6
             7
             8
                           DISTANCE,
                             in.
 1.0
 2.5
 4.8
 8.0
16.8
20.0
22.1
23.8
       PORT LOCATIONS
                         I.D.
                        25 in-.
   T
UPSTREAM
 4.6 ft
 2.2 dd
                                 4.4  ft
                                        UPPER ROOF LEVEL
            DOWNSTREAM
              15.4 ft
               7.5 dd
OFF GAS FROM SCRUBBER
            Figure 4-2.   Entoleter  scrubber  outlet.
                             4-4

-------
for 8 minutes per point, and the sample time was increased to




coincide with the paste mixing operation.






4.3  BAGHOUSE NO. 1



     Total lead, filterable particulate, and condensible  (organic



and inorganic) particulate emissions were measured at the outlet



of Baghouse No. 1, as shown in Figure 4-3.  Two sample ports, 90



degrees apart, were located 5.4 duct diameters downstream and 2.5



duct diameters upstream from the nearest flow disturbances in the



38.1-inch I.D. round stack.   Twenty-eight traverse points, 14



per port, were used to traverse the cross-sectional area of the



stack during each test run.



     For the first two lead tests and one particulate test at



Baghouse No. 1, each point was sampled for 7 minutes, which



yielded a total test time of 196 minutes.  For the third lead



test, each point was sampled for 6 minutes, which yielded a total



test time of 168 minutes.  Sampling time was reduced for the



third lead test to allow completion within time constraints of



process operations.






4.4  BAGHOUSE NO. 2



     Lead and particulate emissions were measured at the outlet



of Baghouse No. 2.  As shown in Figure 4-3, the sampling location



on Baghouse No. 2 is almost identical to that of Baghouse No. 1.



Two sample ports, 90 degrees apart, were located 5.4 duct



diameters downstream and 2.5 duct diameters upstream from the




nearest flow disturbances in the 37.8-inch I.D. round stack.
                              4-5

-------

PLATFORM

1
=6 ft
1
TOP VIEW
                    =8 ft
                    :17 ft
TRAVERSE
POINT NO.
1
2
3
4
5
6
7
8
9
10
11
12
13
14
DISTANCE
BAGHOUSES
NO. 1 AND 3
1.0
2.2
3.8
5.6
7.7
10.3
14.0
24.2
27.9
30.5
32.6
34.4
36.0
37.1
in.
BAGHOUSE
NO. 2
1.0
2.2
3.7
5.5
7.6
10.2
13.8
23.9
27.6
30.2
32.2
34.0
35.6
36.8
                   SIDE VIEW
BAGHOUSES NO. 1 AND 3

DUCT I.D. = 38.1 in.
PORT DIA. = 3 in.
NIPPLE LENGTH =3.5 in.

BAGHOUSE NO. 2

DUCT I.D. = 37.8 in.
PORT DIA. = 3 in.
NIPPLE LENGTH = 3.5 in.

DUCT DIAMETERS
UPSTREAM FROM A
DISTURBANCE - 2.5

DUCT DIAMETERS
DOWNSTREAM FROM
A DISTURBANCE - 5.4

DISTANCE FROM
PLATFORM TO CENTER
OF PORT - 64 in.

DISTANCE FROM TOP
OF RAILING TO THE
PLATFORM - 42 in.
        Figure 4-3.  Baghouses No. 1, 2, and 3  sample  locations.
                                     4-6

-------
Twenty-eight traverse points, 14 per port, were used to traverse



the cross-sectional area of the stack during each test run.



     For the three lead tests and one particulate test at Bag-



house No. 2, each point was sampled for 6 minutes, which yielded



a total test time of 168 minutes.






4.5  BAGHOUSE NO. 3



     Lead and particulate emissions were measured at the outlet



of Baghouse No. 3.  As shown in Figure 4-3, the sampling location



for Baghouse No. 3 is identical to that of Baghouse No. 1.  Two



sample ports, 90 degrees apart, were located 5.4 duct diameters



downstream and 2.5 duct diameters upstream from the nearest flow



disturbances in the 38.1-inch I.D. round stack.  Twenty-eight



traverse points, 14 per port, were used to traverse the cross-



sectional area of the stack during each test run.



     The total sampling time for the initial lead test at Bag-



house No. 3 was 68 minutes.  This test was terminated early



because of operational problems on the processes being tested,



and only 15 points were sampled for 4.5 minutes each.  The sam-



pling time at each point for the second lead test was 7 minutes,



which yielded a total test time of 196 minutes.  For the third



and fourth lead tests, each point was sampled for 5.5 minutes,



which yielded a total test time of 154 minutes.  Sampling times



were reduced for the lead tests to allow completion within time



constraints of process operations.  For the particulate test,




each point was sampled for 5.5 minutes, except for the last




sampling point on one traverse, which was not sampled because the




                               4-7

-------
processes being tested shut down.  Total sampling time for this



test was 149 minutes.






4.6  CARTER-DAY BAGHOUSE



     Lead and particulate emissions were measured at the outlet



of the Carter-Day baghouse, as shown in Figure 4-4.   Two sample



ports, 90 degrees apart, were located 5.1 duct diameters down-



stream and 2.3 duct diameters upstream from the nearest flow



disturbances in the 42-inch I.D. round stack.  Twenty-eight



traverse points, 14 per port, were used to traverse the cross-



sectional area of the stack during each test.



     For the three lead tests and one particulate test at the



Carter-Day baghouse, each point was sampled for 9 minutes, which



yielded a total test time of 252 minutes.  The test and analyti-



cal procedures used at each site are described briefly below.






4.7  VELOCITY AND GAS TEMPERATURE



     A type S pitot tube and an inclined draft gauge manometer



were used to measure the gas velocity pressure (AP).  Velocity



pressures were measured at each sampling point across the duct



according to the procedures outlined in Method 2 of the Federal



Register* to determine an average value.  The temperature at each



sampling point was measured by using a thermocouple and potenti-



ometer.






4.8  MOLECULAR WEIGHT




     Flue gas composition was determined by using procedures




described in Method 3.*  Grab samples were collected at each
 40 CFR 60, Appendix A, Reference Methods 2 and 3, July 1, 1980.




                               4-8

-------
 3-in.
TUBULAR
RAILING
            24-in
            WIDE
   ooooooo  ooooooo
         4  in,
    KICKPLATE,

    GRATE
   GASES  FROM
    BAGHOUSE
      FAN
                                         18  ft
                                     30 ft
                                                      TOP VIEW
DUCT I.D. - 42 in.
PORT DIA. - 4 in.
NIPPLE LENGTH - 3 in.

DUCT DIAMETERS
UPSTREAM FROM A
DISTURBANCE - 2.3

DUCT DIAMETERS
DOWNSTREAM FROM
A DISTURBANCE - 5.1
TRAVERSE
POINT NO.
1
2
3
4
5
6
7
8
9
10
11
12
13
14
DISTANCE,
in.
1.0
2.4
4.2
6.1
8.4
11.3
15.4
26.6
30.7
33.6
35.9
37.8
39.6
41.0
                      SIDE  VIEW
    Figure 4-4.   Carter-Day baghouse sample  location.
                            4-9

-------
test site and analyzed for oxygen and carbon dioxide by using a


Fyrite analyzer.



4.9  PARTICULATE MATTER


     Method 5, as described in the Federal Register, * was used to


measure particulate concentrations at each test location.  All

tests were conducted isokinetically by traversing the cross-


sectional area of the stack and regulating the sample flow rate


relative to the flue gas flow rate as measured by the pitot tube


attached to the sample probe.  A sampling train consisting of a


heated, glass-lined probe, heated 87-mm  (3.5-in.) diameter glass


fiber filter  (Reeve Angel 934 AH), and a series of Greenburg-


Smith impingers was employed for each test.  The nozzle, probe,


and front half portion of the filter holder were acetone-rinsed


at the end of each test.



4.10  LEAD

     The proposed Method 12, as described in the Federal

Register,** was used to measure filterable particulate and total

lead concentrations at each test location.  Before the testing

took place, all glassware was washed with 6 N HNO-, and sealed.


All tests were conducted isokinetically by traversing the cross-


sectional area of the stack and regulating the sample flow rate


relative to the flue gas flow rate as measured by the pitot tube


attached to the sample probe.  A sampling train consisting of a


heated, glass-lined probe, heated 87-mm  (3.5-in.) diameter glass
 *
  40 CFR 60, Appendix A, Reference Method  5, July  1,  1980.
**
  Federal Register, Vol. 45, No. 9, January  14,  1980.



                               4-10

-------
fiber filter (Reeve Angel 934 AH), and a series of Greenburg-



Smith impingers was employed for each test.  The nozzle, probe,



and front-half portion of the filter holder were rinsed first



with acetone and then separately with nitric acid at the end of



each test.
                              4-11

-------

-------
                            SECTION 5
                       SUMMARY OF RESULTS

     This section details results obtained from the emission
testing program.  The results of the testing program are presented
separately for each source sampled.  The emission data presented
for each source includes the flue gas conditions during each
sample run and the lead and particulate concentrations and
emission rates measured.  These values are presented in both
Metric and English units.  In general, the sampling program was
executed as planned, and no major problems occurred either with
test equipment or with sampling activities.  Process operating
conditions monitored for each sample run were characterized as
normal throughout the testing period.
     Appendix A present example calculations.  Appendices B and C
present raw field and laboratory data sheets.  Appendix D details
the sample and analytical procedures used during this test
program.  Appendix E presents equipment calibration procedures
and results.   Appendix F addresses quality assurance considera-
tions pertinent to this test project, and Appendix G lists the
project participants.
     To determine the amount of condensible lead being emitted,
the inorganic fractions of two particulate samples, Runs B2P-1
and CDP-1,  were analyzed for lead content.  These particulate
                               5-1

-------
samples were selected for analysis because they represented the




highest levels of inorganic condensible emissions and should have



represented the highest condensible lead emissions.  The lead



analyses indicated that less than 5 percent of the condensible



particulate emissions were lead.  Because the amount of con-



densible particulate emissions from the other four sources was



lower than the two analyzed for lead, overall condensible lead



emissions from the six sources are likely to be insignificant in



comparison to filterable lead emissions.






5.1  BARTON OXIDE PROCESS BAGHOUSES



     The lead tests were conducted on the Barton Oxide process



Baghouse No. 2, and the particulate test on Barton Oxide process



Baghouse No. 1.  Both baghouses are identical except that they



control emissions from separate but identical Barton Oxide



process lines.



     The maximum variation of the volumetric flow rate between



the two sample runs during the testing period was 5 percent.



The maximum and average concentrations of total lead represented



68 and 54 percent of the filterable particulate concentration.



5.1.1  Flue Gas Conditions and Lead and Particulate Emissions



     Summaries of the measured flue gas conditions and lead and



particulate emissions are presented in Tables 5-1, 5-2, and 5-3.



Volumetric flow rates are expressed in actual cubic meters per



hour (acmh) and actual cubic feet per hour  (acfh) at stack condi-



tions.   Flow rates corrected to standard conditions  [20°C and
                               5-2

-------
                                       TABLE  5-1 .  SUMMARY OF FLUE GAS CONDITIONS AT
                                               BARTON OXIDE BAGHOUSE OUTLETS
01
i
u>
Run No.
2BOL-1
2BOL-2
2BOL-3
1BOP-1
Date
(1981)
6/08
6/08
6/09
6/09
Average
Volumetric flow rate
Actual3
m-Vh
6120
6270
5900
5970
6070
acfh
216200
221500
208200
211000
214200
Standard
dsm3/h
4630
4660
4410
4410
4530
dscfh
163300
164500
155600
155800
159800
Temperature,
°C
93
97
97
99
97
°F
199
207
206
210
206
Moisture,
%
1.05
1.32
1.36
1.82
1.39
02,
%
20.9
20.9
20.9
20.9
20.9
C02,
%
0.0
0.0
0.0
0.0
0.0
            a Volumetric flow rate  in actual cubic meters  per  hour  (m  /h)  and  actual  cubic  feet per hour
              (acfh)  at stack conditions.
            L                                                                O
              Volumetric flow rate  in dry  standard cubic meters per  hour  (dsm  /h)  and dry standard cubic
              feet per hour (dscfh):  Standard conditions  =  20°C  and 760 mmHg  (68°F  and  29.92  in.Hg.).

-------
Ul.
                              TABLE 5-2.   SUMMARY  OF  LEAD  AND  PARTICULATE  EMISSIONS DATA AT
                                               BARTON OXIDE  PROCESS  BAGHOUSES
                                                        (Metric  units)3
Run No.
2BOL-1
2BOL-2
1BOP-1
Date
(1981)
6/08
6/08
6/09
Average
3
Concentration, mg/dsm
Participate
Filterable
12.02
14.70
10.48
11.60
Condensible
Organic
NAb
NA
2.48
2.48
Inorganic
NA
NA
0.548
0.548
Total
lead
3.36
9.94
5.77C
6.65
Mass emission rate, kg/h
Participate
Filterable
0.06
0.07
0.05
0.06
Condensible
Organic
NA
NA
0.01
0.01
Inorganic
NA
NA
0.002
0.002
Total
lead
0.02
0.05
0.03C
0.035
           Concentration in milligrams per dry standard cubic meter (mg/dsm ) (20°C, 760 mmHg), and mass
            emission rate in kilograms per hour (kg/h).

            NA - not available.

            Represents filterable lead only, not included in average.

-------
                           TABLE 5-3.  SUMMARY OF LEAD AND PARTICULATE EMISSIONS DATA AT
                                             BARTON OXIDE PROCESS BAGHOUSES
                                                    (English units)9
Run No.
2BOL-1
2BOL-2
1BOP-1
Date
(1981)
6/08
6/08
6/09
Average
Concentration, gr/dscf
Particulate
Filterable
0.0052
0.0064
0.0046
0.0054
Condensible
Organic
NAb
NA
0.0011
0.0011
Inorganic
NA
NA
0.0002
0.0002
Total
lead
0.0015
0.0043
0.0025C
0.0029
Mass emission rate, Ib/h
Particulate
Filterable
0.122
0.151
0.102
0.125
Condensible
Organic
NA
NA
0.024
0.024
Inorganic
NA
NA
0.005
0.005
Total
lead
0.034
0.102
0.056C
0.068
en
I
en
        Concentration in grains per dry standard cubic foot (gr/dscf) (68°F, 29.92 in.Hg), and mass
        emission rate in pounds per hour (Ib/h).
        NA - not available.
       Represents filterable lead only, not included in average.

-------
760 mm Hg (68°F and 29.92 in.Hg) and 0 percent moisture] are ex-


pressed as dry standard cubic meters per hour (dsm /h) and dry


standard cubic feet per hour (dscfh).   Lead and particulate emis-


sion data are reported on two tables,  one for metric units and


one for English units.  Concentrations are reported as milligrams


per dry standard cubic meter (mg/dsm ) and grains per dry stan-


dard cubic (gr/dscf).   Emission rates are reported as kilograms


per hour  (kg/h) and pounds per hour (Ib/h).  The filterable par-


ticulate data represent material collected in the sample probe


end and on the filter, both of which were heated to approximately


121°C  (250°F).  The condensible organic and inorganic fractions


represent material that passed through the filter and was col-


lected by the impinger section of the sampling train at approxi-


mately 20°C  (68°F).  The total lead data represent combined fil-


terable and condensible lead fractions.


     During the testing period the volumetric flow rate averaged

        3
4530 dsm /h  (159,800 dscfh), and the average stack gas tempera-


ture was  97°C  (206°F).  The moisture content averaged 1.39


percent; and the oxygen and carbon dioxide contents were 20.90


and 0.0 percent, respectively.


     The  filterable particulate concentration averaged 11.60


mg/dsm  (0.0054 gr/dscf), and the corresponding mass emission


rate was  0.06 kg/h (0.125 Ib/h).  Organic and inorganic concen-


trations were 2.48 mg/dsm   (0.0011 gr/dscf) and 0.548 mg/dsm


(0.0002 gr/dscf), and corresponding mass emission rates were


0.01 kg/h (0.024 Ib/h) and 0.002 kg/h  (0.005 Ib/h).  The average


                               5-6

-------
lead concentration was 6.65 mg/dsm   (0.0029 gr/dscf), and the



average mass emission rate was 0.035 kg/h  (0.068 Ib/h).



     The results of the sample analysis for Run 2BOL-3 showed the



measured lead and particulate concentrations to be erroneous.



For this reason the lead and particulate analysis results from



this run were not reported.






5.2  ENTOLETER SCRUBBER OUTLET



     Emissions from the three paste mixers, the mixed paste



quality test booth, and the calcium lead alloy pasting machine,



and off-bear station are controlled by the Entoleter scrubber.



     Because all of the paste mixers charge the same amount of



PbO per batch (2400 Ib), their lead emissions should be similar.



Particulate emissions may be higher from the calcium lead alloy



and antimony lead alloy negative paste mixers because an expander



is charged in these mixers along with the other materials neces-



sary to produce positive paste.  The paste mixing operations and



the off-bear station should contribute most of the particulate



and lead emissions controlled by the Entoleter scrubber.



     During the test period, the maximum variation in the volu-



metric flow rates between any sample runs was 5.5 percent.  The



maximum and average concentrations of total lead represented 42



and 16 percent of the filterable particulate emissions.



5.2.1  Flue Gas Conditions and Lead and Particulate Emissions



     Tables 5-4,  5-5,  and 5-6 present summaries of measured flue




gas,  lead,  and particulate emissions, respectively.  During the
                               5-7

-------
                                         TABLE 5-4.  SUMMARY OF FLUE GAS CONDITIONS AT
                                                  ENTOLETER SCRUBBER OUTLET
tn
I
oo
Run No.
ESL-1
ESL-2
ESL-3
ESP-1
Date
(1981)
6/08
6/09
6/10
6/09
Average
Volumetric flow rate
Actual3
m3/h
18410
19170
18490
19670
18940
acfh
650300
677000
652900
694800
668700
Standard*5
dsm3/h
16360
16970
16500
17310
16780
dscfh
577600
599400
582600
611300
592700
Temperature,
°C
32
34
32
34
33
°F
90
93
90
94
92
Moisture,
%
2.78
3.00
3.06
3.53
3.09
02,
%
20.90
20.90
20.90
20.90
20.90
C02,
%
0.0
0.0
0.0
0.0
0.0
            a Volumetric flow rate in actual cubic meters per hour (m /h) and actual cubic feet per  hour

              (acfh) at stack conditions.
            h                                                                ^
              Volumetric flow rate in dry standard cubic meters per hour  (dsm /h) and dry standard cubic
              feet per hour  (dscfh):  Standard conditions = 20°C and 760 rnrnHg (68°F and 29.92 in.Hg.).

-------
                              TABLE .5-5.  SUMMARY OF LEAD AND PARTICULATE  EMISSIONS  DATA
                                               ENTOLETER SCRUBBER OUTLET
                                                    (Metric units)3
Run No.
ESL-1
ESL-2
ESL-3
ESP-1
Date
(1981)
6/08
6/09
6/10
6/09
Average
Concentration, mg/dsm3
Particulate
Filterable
2.05
11.98
2.15
6.91
5.77
Condensible
Organic
NAb
NA
NA
0.62
0.62
Inorganic
NA
NA
NA
0.088
0.088
Total
lead
0.498
1.263
0.899
NA
0.887
Mass emission rate, kg/h
Particulate
Filterable
0.03
0.20
0.04
0.12
0.10
Condensible
Organic
NA
NA
NA
0.01
0.01
Inorganic
NA
NA
NA
0.00
0.00
Total
lead
0.01
0.02
0.01
NA
0.01
en
I
vo
           Concentration in  milligrams  per  dry  standard  cubic meter (mg/dsm )(20°C, 760 mmHg), and mass
           emission rate in  kilograms  per  hour  (kg/h).
           NA -  not available.

-------
                         TABLE  5-6.  SUMMARY OF LEAD AND PARTICULATE EMISSIONS DATA
                                          ENTOLETER SCRUBBER OUTLET
                                                (English units)3
Run No.
ESL-1
ESL-2
ESL-3
ESP-1
Date
(1981)
6/08
6/08
6/10
6/09
Average
Concentration, gr/dscf
Particulate
Filterable
0.0009
0.0052
0.0009
0.0030
0.0025
Condensible
Organic
NAb
NA
NA
0.0003
0.0003
Inorganic
NA
NA
NA
0. 0000
0.0000
Total
lead
0.0002
0.0006
0.0004
NA
0.0004
Mass emission rate, Ib/h
Particulate
Filterable
0.074
0.448
0.078
0.264
0.216
Condensible
Organic
NA
NA
NA
0.024
0.024
Inorganic
NA
NA
NA
0.003
0.003
Total
lead
0.018
0.047
0.033
NA
0.033
I
!-•
O
     Concentration  in arains per dry standard cubic foot (gr/dscf)(68°F, 29.92  in.Hg),  and  mass  emis-
     sion rate  in pounds  per hour  (Ib/h).

     JNA - not available.

-------
testing period the average volumetric flow rate was 16,780 dsm /h



(592,700 dscfh), and the moisture content was 3.09 percent.  The



oxygen and carbon dioxide contents were 20.9 and 0.0 percent, and



the average flue gas temperature was 33°C  (92°F).



     The filterable particulate concentration averaged 5.77



mg/dsm  (0.0025 gr/dscf) and the mass filterable emission rate



averaged 0.10 kg/h (0.216 Ib/h).  The organic and inorganic



concentrations were 0.62 mg/dsm3 (0.0003 gr/dscf) and 0.088



mg/dsm  (0.00004 gr/dscf), and the corresponding mass emission



rates were 0.01 kg/h (0.024 Ib/h) and 0.001 kg/h (0.003 Ib/h).



The total lead concentration averaged 0.887 mg/dsm  (0.0004



gr/dscf),  and the mass emission rate was 0.01 kg/h  (0.033 Ib/h).






5.3  BAGHOUSE NO. 1 OUTLET



     Baghouse No. 1 controls emissions from the two automatic



stacking machines and off-bear stations, two hand stacking sta-



tions, two antimony lead alloy pasted plate off-bear stations,



three automatic parting machines and off-bear stations, and the



manually operated parting machine.   Because so many different



processes are controlled by this baghouse, it is not possible to



determine which sources produce the most particulate and lead



emissions.



     During the testing period, the maximum variation in the



volumetric flow rates between any sample runs was 5.8 percent.



The maximum and average concentrations of total lead represented




45 and 43  percent of the filterable particulate emissions.
                              5-11

-------
     Tables 5-7, 5-8, and 5-9 present summaries of measured flue



gas conditions and emissions data.  The average volumetric flow



rate was 42,670 dsm3/h (1,506,700 dscfh), and the average flue



gas temperature was 36°C (96°F).   The moisture content averaged



1.13 percent, and the oxygen and carbon dioxide content averaged



20.9 and 0.0 percent, respectively.



     The filterable particulate concentration averaged 3.57



mg/dsm  (0.0013 gr/dscf), and the mass emission rate averaged



0.16 kg/h  (0.337 Ib/h).  Organic and inorganic concentrations



were 0.500 mg/dsm  (0.0002 gr/dscf) and 0.274 mg/dsm   (0.0001



mg/dscf),  and corresponding mass emission rates were 0.02 kg/h



(0.049 Ib/h) and 0.01 kg/h  (0.027 Ib/h).  The lead concentration



averaged 1.56 mg/dsm  (0.0007 gr/dscf), and the corresponding



average mass emission rate was 0.07 kg/h  (0.144 Ib/h).






5.4  BAGHOUSE NO. 2 OUTLET



     Baghouse No. 2 controls emissions originating from two hand-



stacking stations and seven MAC machines  for antimony  lead alloy



batteries.



     It appears that emissions from the seven MAC machines should



contribute most of the particulate lead emissions controlled by



this baghouse.



     During the testing period, the maximum variation  in the



volumetric flow rates between any sample  runs was 2.7  percent.



The maximum and average concentrations of total lead represented




31 and 22 percent of the filterable particulate emissions.
                              5-12

-------
                                         TABLE 5-7.   SUMMARY OF FLUE GAS CONDITIONS AT
                                                      BAGHOUSE NO.  1 OUTLET
Ul

H
U>
Run No.
BIL-1
BIL-2
BIL-3
BIP-1
Date
(1981)
6/10
6/10
6/11
6/10
Average
Volumetric flow rate
J\ctuala
nr/h
46C90
46270
46610
48930
46970
acfh
1627500
1634100
1645900
1728000
1658900
Standard13
dsm^/h
41750
42P80
42340
44300
42670
dscfh
1474200
1492900
1495100
1 564 500
1506700
Temperature,
°C
35
36
35
36
36
°F
95
97
94
97
96
Moisture,
%
1.32
0.30
1.66
1.23
1.13
02,
%
20.90
20.90
20.90
20.90
20.90
C02,
%
0.0
0.0
0.0
0.0
0.0
                                                                       A
              3 Volumetric flow rate in actual  cubic meters per hour (m /h) and actual cubic feet per
                hour (acfh) at stack conditions.
              h                                                                ^
                Volumetric flow rate in dry standard cubic meters per hour (dsm /h) and dry standard cubic
                feet per hour (dscfh):   Standard  conditions = 20°C and 760 mmHg (68°F and 29.92 in.Hg.).

-------
                    TABLE 5-8.   SUMMARY  OF  LEAD AND  PARTICULATE  EMISSIONS DATA AT
                                        BAGHOUSE  NO.  1  OUTLET
                                           (Metric units)3
Run No.
BIL-1
BIL-2
BIL-3
BIP-1
Date
(1981)
6/10
6/10
6/10
6/10
Average
3
Concentration, mg/dsn
Particulate
Filterable
4.19
2.53
3.16
4.1
3.57
Condensible
Organic
NAb
NA
NA
0.500
0.500
Inorganic
NA
NA
NA
0.274
0.274
Total
lead
1.84
1.41
1.42
NA
1.56
Mass emission rate, kg/h
Particulate
Filterable
0.18
0.11
0.13
0.20
0.16
Condensible
Organic
NA
NA
NA
0.02
0.02
Inorganic
NA
NA
NA
0.01
0.01
Total
lead
0.08
0.06
0.06
NA
0.07
Concentration in milligrams per dry standard  cubic meter  (mg/dsm  )  (20°C,  760 mmHg), and  mass
 emission rate in kilograms per hour (kg/h).
 NA - not available.

-------
                         TABLE 5-9.  SUMMARY OF LEAD AND PARTICULATE EMISSIONS DATA AT
                                            BAGHOUSE NO. 1 OUTLET
                                               (English units)3
Run No.
BIL-1
BIL-2
BIL-3
BIP-1
Date
(1981)
6/10
6/10
6/11
6/10
Average
Concentration, gr/dscf
Particulate
Filterable
0.0018
0.0011
0.0014
0.0019
0.0013
Condensible
Organic
NAb
NA
NA
0.0002
0.0002
Inorganic
NA
NA
NA
0.0001
0.0001
Total
lead
0.0008
0.0006
0.0006
NA
0.0007
Mass emission rate, Ib/h
Particulate
Filterable
0.386
0.236
0.295
0.430
0.337
Condensible
Organic
NA
NA
NA
0.049
0.049
Inorganic
NA
NA
NA
0.027
0.027
Total
lead
0.169
0.131
0.132
NA
0.144
Ul
I
      Concentration  in  grains  per dry standard cubic foot  (gr/dscf)  (68°F,  29.92  in.Hg),  and  mass
      emission  rate  in  pounds  per hour  (Ib/h).
     5NA  -  not  available.

-------
5.4.1  Flue Gas Conditions and Lead and Particulate Emissions



     Tables 5-10, 5-11, and 5-12 present summaries of the mea-



sured flue gas conditions and emission data.  The average volu-



metric flow rate was 45,160 dsm /h (1,594,700 dscfh), and the



average flue gas temperature was 40°C  (103°F).  The moisture



content was 1.63 percent, and the oxygen and carbon dioxide con-




tents were 20.9 and 0.0 percent, respectively.



     The filterable particulate concentration averaged 2.363



mg/dsm  (0.0010 gr/dscf), and the mass emission rate averaged



0.11 kg/h  (0.236 Ib/h).  The organic and inorganic concentrations



were 0.543 mg/dsm   (0.0002 gr/dscf) and 0.645 mg/dsm  (0.0003



gr/dscf),  and the corresponding mass emission rates were 0.02



kg/h (0.055 Ib/h) and  0.03 kg/h (0.065 Ib/h).  The lead concen-



tration averaged 0.525 mg/dsm   (0.0002 gr/dscf), and the corre-



sponding average emission rate was 0.02 kg/h  (0.052 Ib/h).






5.5  BAGHOUSE NO. 3 OUTLET



     Baghouse No. 3 controls emissions originating from 10 Tiegel



machines and Tiegel Intercell Line No. 1.  The Tiegel machines



are used to burn elements of different types of batteries, which



means the  size and number of elements per battery vary.  The



amount of  lead used also varies with the type of battery element



being burned.  Lead consumption over a long period of time should



be fairly consistent for the Tiegel machines, despite the type of



element being burned because the production rate for batteries



using fewer or smaller size elements should be greater than that
                              5-16

-------
                                       TABLE 5-10.  SUMMARY OF FLUE GAS CONDITIONS AT
                                                   BAGHOUSE NO.  2 OUTLET
en
I
Run No.
B2L-1
B2L-2
B2L-3
B2P-1
Date
(1981)
6/11
6/11
6/12
6/12
Average
Volumetric flow rate
Actual9
nr/h
50320
49880
50420
51300
50480
acfh
1777100
1761 500
1780400
1810500
1782400
Standard
dsm3/h
45230
44490
45160
45760
45160
dscfh
1597200
1570900
1594800
1615900
1594700
Temperature,
°C
39
42
38
39
40
°F
102
108
101
101
103
Moisture,
%
1.59
1.29
1.67
1.98
1.63
02,
%
20.90
20.90
20.90
20.90
20.90
C02,
%
0.0
0.0
0.0
0.0
0.0
           a Volumetric flow rate in actual  cubic meters per hour (m /h) and actual cubic feet per
             hour (acfh) at stack conditions.

             Volumetric flow rate in dry standard cubic meters per hour (dsm /h) and dry standard cubic
             feet per hour (dscfh):   Standard  conditions = 20°C and 760 mmHg (68°F and 29.92 in.Hg.).

-------
                             TABLE 5-11.  SUMMARY OF LEAD AND PARTICULATE EMISSIONS DATA AT
                                                  BAGHOUSE NO. 2 OUTLET
                                                     (Metric units)3
Run No.
B2L-1
B2L-2
B2L-3
B2P-1
Date
(1981)
6/11
6/11
6/12
6/12
Average
Concentration, mg/dsm
Particulate
Filterable
3.112
1.542
1.487
3.312
2.363
Condensible
Organic
NAb
NA
NA
0.543
0.543
Inorganic
NA
NA
NA
0.645
0.645
Total
lead
0.605
0.477
0.463
0.554
0.525
Mass emission rate, kg/h
Particulate
Filterable
0.14
0.07
0.07
0.15
0.11
Condensible
Organic
NA
NA
NA
0.02
0.02
Inorganic
NA
NA
NA
0.03
0.03
Total
lead
0.03
0.02
0.02
0.02
0.02
Ul

(-•
00
           Concentration in milligrams per dry standard cubic meter (mg/dsm3) (20°C, 760 mmHg), and mass
           emission rate in kilograms per hour (kg/h).

           NA -  not available.

-------
                        TABLE  5-12.  SUMMARY OF LEAD AND PARTICULATE EMISSIONS DATA AT
                                           BAGHOUSE NO. 2 OUTLET
                                               (English units) a
Run No.
B2L-1
B2L-2
B2L-3
B2P-1
Date
(1981)
6/11
6/11
6/12
6/12
Average
Concentration, gr/dscf
Particulate
Filterable
0.0014
0.0007
0.0006
0.0014
0.0010
Condensible
Organic
NAb
NA
NA
0.0002
0.0002
Inorganic
NA
NA
NA
0.0003
0.0003
Total
lead
0.0003
0.0002
0.0002
0.0002
0.0002
Mass emission rate, Ib/h
Particulate
Filterable
0.310
0.151
0.148
0.334
0.236
Condensible
Organic
NA
NA
NA
0.055
0.055
Inorganic
NA
NA
NA
0.065
0.065
Total
lead
0.060
0.047
0.046
0.055
0.052
vo
     Concentration  in  grains  per  dry  standard cubic  foot  (gr/dscf)  (68°F,  29.92  in.Hg),  and mass
     emission  rate  in  pounds  per  hour (Ib/h).

    JNA  -  not  available.

-------
for the larger batteries that consume more lead and would there-


fore increase the lead consumption rate on a hourly basis.


     During the test period, the maximum variation in the volu-


metric flow rates between any sample runs was 3.9 percent.  The


maximum and average concentrations of total lead represented 47


and 29 percent of the filterable particulate emissions.


5.5.1  Flue Gas Conditions and Lead and Particulate Emissions


     Tables 5-13, 5-14, and 5-15 present summaries of the mea-


sured flue gas conditions and emission data.  The average volu-

                               -3
metric flow rate was 51,220 dsm /h  (1,808,900 dscfh), and the


average flue gas temperature was 32°C (90°F).  Moisture content


was 1.06 percent, and oxygen and carbon dioxide contents were


20.90 and 0.0 percent, respectively.


     The filterable particulate concentration averaged 2.47


mg/dsm  (0.0011 gr/dscf), and the mass emission rate was 0.13


kg/h (0.279 Ib/h).  Organic and inorganic concentrations were


0.909 mg/dsm3  (0.0004 gr/dscf) and  0.273 mg/dsm3  (0.0001 gr/dscf),


and corresponding mass emission rates were 0.05 kg/h  (0.103 Ib/h)


and 0.01 kg/h  (0.031 Ib/h).  The lead concentration averaged


0.729 mg/dsm   (0.0003 gr/dscf), and the average emission rate was


0.04 kg/h (0.082 Ib/h).



5.6  CARTER-DAY BAGHOUSE OUTLET


     The Carter-Day baghouse controls emissions originating from


three wrapping process lines, four  calcium lead alloy MAC


machines, two calcium lead alloy MAC melting pots, the automotive
                                5-20

-------
                                         TABLE 5-13.   SUMMARY OF FLUE GAS CONDITIONS AT

                                                    BAGHOUSE NO. 3 OUTLET
I
NJ
Run No.
B3L-1C
B3L-2
B3L-3
B3L-4
B3P-1
Date
(1981)
6/09
6/10
6/10
6/11
6/11
Average
Volumetric flow rate
.Actual3
mj/h
55140
55490
55530
56390
56710
56030
acfh
1947200
1959600
1961000
1991400
2002700
1978700
Standard13
dsm3/h
49680
50880
50770
51690
51560
51220
dscfh
1754400
1796700
1792900
1825200
1820700
1808900
Temperature,
°C
31
30
32
32
35
32
°F
87
86
90
90
95
90
Moisture,
%
2.07
0.97
1.03
1.18
1.04
1.06
02»
%
20.90
20.90
20.90
20.90
20.90
20.90
C02,
%
0.0
0.0
0.0
0.0
0.0
0.0
            a Volumetric flow rate in actual cubic meters per hour (m /h) and actual cubic feet per hour

              (acfh) at stack conditions.
            u                                                                O
              Volumetric flow rate in dry standard cubic meters per hour (dsm /h) and dry standard cubic

              feet per hour (dscfh):   Standard conditions = 20°C and 760 mmHg (68°F and 29.92 in.Hg.).

            c Test aborted due to process shutdown; results not included in the average.

-------
                         TABLE  5-14.
SUMMARY OF LEAD AND PARTICULATE EMISSIONS DATA AT
        BAGHOUSE NO.  3 OUTLET
           (Metric units)3
Run No.
B3L-lb
B3L-2
B3L-3
B3L-4
B3P-1
Date
(1981)
6/09
6/10
6/10
6/11
6/11
Average
3
Concentration, mg/dsm
Particulate
Filterable
2.826
1.787
1.989
2.890
3.199
2.47
Condensible
Organic
NAC
NA
NA
NA
0.909
0.909
Inorganic
NA
NA
NA
NA
0.273
0.273
Total
lead
0.880
0.441
0.938
0.808
NA
0.729
Mass emission rate, kg/h
Particulate
Filterable
0.14
0.09
0.10
0.15
0.16
0.13
Condensible
Organic
NA
NA
NA
NA
0.05
0.05
Inorganic
NA
NA
NA
NA
0.01
0.01
Total
lead
0.04
0.02
0.05
0.04
NA
0.04
(Jl
I
|NJ
fO
     Concentration  in milligrams per dry standard cubic meter  (mg/dsm  )  (20°C, 760 mmHg),  and  mass
      emission rate  in kilograms per hour (kg/h).

      Test aborted due to  process shutdown; results not included in the average.

     CNA - not available.

-------
                        TABLE  5-15.
SUMMARY OF LEAD AND PARTICULATE EMISSIONS DATA AT
      BAGHOUSE NO. 3 OUTLET
         (English units)3
Run No.
B3L-lb
B3L-2
B3L-3
B3L-4
B3P-1
Date
(1981)
6/09
6/10
6/10
6/11
6/11
Average
Concentration, gr/dscf
Particulate
Filterable
0.0012
0.0008
0.0009
0.0013
0.0014
0.0011
Condensible
Organic
NAC
NA
NA
NA
0.0004
0.0004
Inorganic
NA
NA
NA
NA
0.0001
0.0001
Total
lead
0.0004
0.0002
0.0004
0.0004
NA
0.0003
Mass emission rate, Ib/h
Particulate
Filterable
0.309
0.200
0.223
0.329
0.364
0.279
Condensible
Organic
NA
NA
NA
NA
0.103
0.103
Inorganic
NA
NA
NA
NA
0.031
0.031
Total
lead
0.096
0.049
0.105
0.092
NA
0.082
Ul
I
to
    Concentration in grains per dry standard cubic foot (gr/dscf) (68°F, 29.92 in.Hg), and mass
    emission rate 1n pounds per hour (Ib/h).
   5Test aborted due to a process shutdown; results not included in the average.
    NA - not available.

-------
battery and heavy-duty battery inspection stations, the antimony



and calcium alloy battery repair stations, and Tiegel Intercell



Line No. 2.



     Because so many different processes are controlled by the



Carter-Day baghouse, it was not possible to determine which



sources produce the most particulate and lead emissions.



     During the testing period, the maximum variation in the



volumetric flow rates between any sample runs was 5.5 percent.



However, throughout the testing period flue gas emissions out of



the bottom of the stack were observed.  The configuration of the



stack prohibited measurement of the velocity of these flue gas



emissions.  The maximum and average concentrations of total lead



represented 21 and 11 percent of the filterable particulate



emissions.



5.6.1  Flue Gas Conditions and Lead and Particulate Emissions



     Tables 5-16, 5-17, and 5-18 present summaries of the mea-



sured flue gas conditions and emission data.  The average volu-



metric flow rate was 46,510 dsm /h  (1,642,400 dscfh), and the



average flue gas temperature was 35°C  (94°F).  The moisture con-



tent was 2.38 percent, and the oxygen and carbon dioxide contents



were 20.90 and 0.0 percent, respectively.



     The filterable particulate concentration averaged 1.455



mg/dsm  (0.0006 gr/dscf), and the corresponding mass emission



rate was 0.07 kg/h  (0.150 Ib/h).  Organic and inorganic concen-



trations were 0.524 mg/dsm   (0.0002 gr/dscf) and 0.821 mg/dsm



(0.004 gr/dscf), and corresponding mass emission rates were
                               5-24

-------
                              TABLE  5-16.
                                     SUMMARY OF FLUE GAS CONDITIONS AT
                                     CARTER DAY BA6HOUSE OUTLET
Ul
i
N)
Ul
Run No.
CDL-1
CDL-2
CDL-3
CDP-1
Date
(1981)
6/08
6/10
6/11
6/08
Average
Volumetric flow rate
o Actual9
nT/h
52050
51480
50920
54170
52150
acfh
1838200
1817900
1798200
1912900
1841800
Standard
dsm-Vh
46610
46000
45380
48040
46510
dscfh
1646000
1624300
1602600
1696600
1642400
Temperature,
°C
35
32
34
37
35
r op
94
90
93
99
94
Moisture,
%
1.44
3.05
3.50
1.51
2.38
0?
20.90
20.90
20.90
20.90
20.90
C02,
%
0.0
0.0
0.0
0.0
0.0
a Volumetric flow rate in actual cubic meters per hour (m /h) and actual cubic feet per
  hour (acfh) at stack conditions.
i                                                                 O
  Volumetric flow rate in dry standard cubic meters per hour (dsm /h) and dry standard cubic
  feet per hour (dscfh):  Standard conditions = 20°C and 760 mrnHg (68°F and 29.92 in.Hg.).

-------
                        TABLE  5-17. SUMMARY OF LEAD AND PARTICULATE EMISSIONS DATA AT
                                          CARTER-DAY BAGHOUSE OUTLET
                                                (Metric units)3
Run No.
CDL-1
CDL-2
CDL-3
CDP-1
Date
(1981)
6/08
6/10
6/11
6/08
Average
Concentration, mg/dsm3
Particulate
Filterable
0.891
1.887
1.104
1.939
1.455
Condensible
Organic
NAb
NA
NA
0.524
0.524
Inorganic
NA
NA
NA
0.821
0.821
Total
lead
0.187
0.135
0.124
0.204
0.163
Mass emission rate, kg/h
Particulate
Filterable
0.04
0.09
0.05
0.09
0.07
Condensible
Organic
NA
NA
NA
0.03
0.03
Inorganic
NA
NA
NA
0.04
0.04
Total
lead
0.01
0.01
0.01
0.01
0.01
to
     Concentration in milligrams per dry standard cubic meter (mg/dsm )  (20°C, 760 mmHg), and mass
      emission rate in kilograms per hour (kg/h).
     °NA - not available.

-------
                        TABLE 5-18.  SUMMARY OF LEAD AND PARTICIPATE EMISSIONS DATA AT
                                          CARTER-DAY BAGHOUSE OUTLET
                                                (English units)3
Run No.
CDL-1
CDL-2
CDL-3
CDP-1
Date
(1981)
6/08
6/10
6/11
6/08
Average
Concentration, gr/dscf
Particulate
Filterable
0.0004
0.0008
0.0005
0.0008
0.0006
Condensible
Organic
NAb
NA
NA
0.0002
0.0002
Inorganic
NA
NA
NA
0.0004
0.0004
Total
lead
0.0001
0.0001
0.0001
0.0001
0.0001
Mass emission rate, Ib/h
Particulate
Filterable
0.092
0.191
0.110
0.205
0.150
Condensible
Organic
NA
NA
NA
0.055
0.055
Inorganic
NA
NA
NA
0.087
0.087
Total
lead
0.019
0.014
0.012
0.021
0.017
\J
      Concentration in grains oer dry standard cubic foot (gr/dscf) (68°F, 29.92 in.Hg), and mass
      emission rate in pounds per hour (Ib/h).
     bNA - not available.

-------
0.03 kg/h (0.055 Ib/h) and 0.04 kg/h (0.087 Ib/h).  The lead



concentration averaged 0.163 mg/dsm  (0.0001 gr/dscf), and the



corresponding mass emission rate was 0.01 kg/h  (0.017 Ib/h).
                               5-28

-------
                            SECTION 6



                        QUALITY ASSURANCE






     Quality assurance is one of the main facets of stack sam-



pling because the end product of testing is to produce repre-



sentative emission results.  Quality assurance guidelines provide



detailed procedures and actions necessary for defining and pro-



ducing acceptable data.  Four documents were used in this test



program to provide the required guidance to help insure the col-



lection of acceptable data and determine when data quality is



unacceptable.  These documents are the source-specific test plan



prepared by PEDCo and reviewed by Region VII EPA; the EPA Quality



Assurance Handbook Volume III, EPA-600/4-77-027b; the draft PEDCo



Environmental Emission Test Quality Assurance Plan; and the PEDCo



Environmental Laboratory Quality Assurance Plan.  The last two



quality assurance plans are PEDCo1s general guideline manuals,



which define the standard operating procedures followed by the



company's emission testing and the laboratory groups.



     Appendix F provides more detail on the quality assurance



procedures, including QA objectives; data reduction; quality



control checks; performance and system audits; preventive main-



tenance;  precision, accuracy, and completeness; corrective



action; and quality assurance reports to management.
                               6-1

-------
     Relative to this specific test program, the following steps

were taken to ensure that quality data were obtained by the test-

ing and analytical procedures.

     0    Calibration of field sampling equipment.  (Calibration
          guidelines are described in more detail in Appendix E.)

     0    Train configuration and calculation checks.

     0    Onsite quality assurance checks, such as leak checks
          on the sample train and pitot tube.

     0    Use of designated analytical equipment and sampling
          reagents.

     Table 6-1 lists sampling equipment used to conduct particu-

late and lead tests, along with calibration guidelines and

limits.  In addition to the pre- and post-test calibration, a

field audit was performed on the dry gas meters by using critical

orifices calibrated and supplied by the EPA.  The audit results

in Table 6-2 show that all dry gas meters used for this series

were within limitations stipulated in EPA Method 5.  Dry gas

meter performance test procedures and field audit sheets are

shown in Figures 6-1 through  6-9.  In addition to the pre-test

calibration, a field audit was performed on the digital tempera-

ture indicators by using a device to simulate millivolt inputs

comparable to thermocouple voltages.  Onsite digital inidicator

audit sheets are shown in Figures 6-10 through  6-12.  All digital

indicator readings fell within the allowable range.

     Between runs, preliminary calculation checks were performed

to verify isokinetic sampling rates and to compare moisture

contents, flow rates, and other parameters with expected values.

These checks indicated that the tests were being conducted

properly.
                               6-2

-------
                                  TABLE 6-1.   FIELD EQUIPMENT CALIBRATION
Equipment
Meter box
Meter box
Meter box
Meter box
Pi tot tube
Pi tot tube
Pitot tube
Pi tot tube
Thermocouple
Thermocouple
I.D.
No.
FB-2
FB-3
FB-6
FB-10
017
032
179
180
127
128
Cal ibrated
against
Wet test meter



Standard pi tot tube



ASTM reference
thermometer

Allowable
deviation
AY prea + 0.020
AH@, +0.15
AY postb + 0.05



A Cp + 0.01



+ 1.5%

Actual
deviation
-0.005
-0.07
+0.002
-0.003
-0.09
-0.007
+0.001
-0.06
-0.003
+0.005
-0.10
-0.004
0.01
0.003
0.01
0.003
+0.87
-0.87
Within
allowable
1 imits
/
/
/
/
/
/
/
/
/
/
/
/
/
/
/
/
/
/
Comments
Y~ pre = 1 . 003
7 post = 1.005
Y pre = 1.018
T post = 1.011
Y" pre = 0.973
Y" post = 0.970
7 pre = 1 . 044
Y" post = 1.040
Cp = 0.82
Cp = 0.80
Cp = 0.82
Cp = 0.81


(continued)
 Allowable deviation AY pretest = +0.02 Y pretest.
'Allowable deviation AY post-test = +0.05 Y pretest.

-------
TABLE 6-1 (continued)
Equipment
Thermocouple
Thermocouple
Thermocouple
Digital
indicator



Trip balance
Barometer

Dry gas
thermometer







I.D.
No.
129
133
174
126
207
262
221

194


FB-2


FB-3

FB-6

FB-10

Cal i bra ted
against



Mill ivolt signals




Type S weights
N3S-traceable
barometer
Reference thermom-
eter type ASTM 2F
or 3F






Allowable
deviation



0.5%




+0.5 g
0.20 in. Hg
post-test
+5°F








Actual
deviation
+0.87
-0.50
-0.72





0.10 g
O.OU
in. Hg
I 3.1°F
0 4.0°F

I 3.0°F
0 2.7°F
I 1.0°F
0 3.0°F
I 2.0°F
0 2.0°F
Within
allowable
1 imits
/
/
/
/
/
/
/

/
/

/
J

/
/
/
^
/
/
Comments



Actual deviation is
an average of eight
temperature points;
cal ibrated by manu-
facturer



I = inlet thermometer
0 = outlet thermometer







(continued)

-------
    TABLE 6-1  (continued)
Equipment
Probe nozzle









I.D.
No.
3-108
4-102
4-116
4-116
4-117
4-117
4-122
4-122
5-104
5-104
Cal ibrated
against
Cali per









Allowable
deviation
Dn + 0.004 in.









Actual
deviation
0.001
0.002
0.002
0.003
0.001
0.001
0.001
0.002
0.001
0.003
Within
al lowable
limits
/
/
/
/
/
/
/
/
/
/
Comments










CM
I

-------
TABLE 6-2.   DRY GAS METER AUDITS
Meter box No.
FB-2
FB-2
FB-3
FB-3
FB-6
FB-6
FB-10
FB-10
FB-10
Cal ibrated against
Critical orifice No. 3
Critical orifice No. 4
Critical orifice No. 5
Critical orifice No. 5
Critical orifice No. 4
Critical orifice No. 3
Critical orifice No. 4
Critical orifice No. 4
Critical orifice No. 5
Deviation, %
+ 1.4
+ 3.1
+ 0.9
+ 1.6
+ 0.6
+ 1.5
+ 1.9
+ 2.2
+ 2.2
              6-6

-------
                                          AUDIT  REPORT SAMPLE METER BOX
Date
Barooteteric pressure (P.   »  in Hg  )_
Orifice nuaiber     3
Orifice K factor
               J ,
                                 to
                                                    Client
                                                    Meter  box  number /-

                                                    Pretest Y

                                                    Aud i to r   J

Orifice
nanometer
reading
AH
in H20
J.3*
Dry gas
meter
reading
V /V
V*f
ft
/???£>
He, 7J*
Dry gas
meter
V
ft3
,M
Temi
Ambient
T /T
ai af
°F
tf
trr
Average
T
a
°F
rr;
eratures
Inlet
T i
mi
°F
Z 1
?w
V
•sta
ft3
A?. 6 3
V
ra
act
ft3
—
Percent
error
7V
•O -*, - ' i
^ . , A , M - ^ / /I
                                                                        {,'/
  Std
V
 *«ct
V
 "•td
V
 Vt

error
( 17.647 )( V  )( Y )( P.   + AH/13.6 )/( T  +  460  )
             m          bar                m
                         )/( T  + 460 )
                                       *
  ( 1203 )( 0  )( K  )(

  ( 17.647  )( /3.e>3J

• ( 1203 )( / >">*•
( v     - v     )( 100 )/( v      ) -  (r,/1??  )(  100
   *std    "act             "act
                                      Figure 6-1.   Audit report sample meter box.

-------
                                                 AUDIT REPORT SAMPLE METER BOX
             Date
             Baromateric Pressure  (Pbar» in Hg)
             Orifice number	V
             Orifice K factor
                 T.^o vr'Q
                                                             Client   f'M
                                                             Meter box number
                                                             Pretest Y   /', o
                                                                                     AH0
                                                                          _
                                                             Auditor   \J  I
                                                                                   /, 7 £
Orifice
manometer
reading
AH
in H20
y.f
Y
percent
error
fi/7.
deviation
in H20

i
CO
 U.td
<17.647)(V )(Y)(P.    -f AH/13.6)/(T  + 460)
          m      oar              m
         act
       Percent error
        (1203)(0)(K)(Pbar)/(Ta
                                        460)
                (V.
              - V
                                m
                                              m
                                           )
                          "act           act
AH® deviation = [(0.0317)(AH)/(Pbar)(Tm -f 460)][(Ta
      « (17.647H/ 3 . ££

      - (1203)(/£. o^.
Percent error -[(£.£ J T J
AH® deviation - [(0.0317)(_ .

                                                             460)(0)/(Vm   )]
                                                                        act
                         (^ ' • ^ Jr^J](100%)/( A . £ £•£ J
                         )/(_ _ . ___ )( ___ . _ _)][(
                                                                      _ J- . /_
                                                                      . _ _)(
                                                                                                )/(,
                                            Figure  6-2.  Audit report  sample meter  box.

-------
             Date
                                        AUDIT REPORT SAMPLE METER  BOX

                                        	          Client
      Barometeric Pressure (P.   ,  in
      Orifice number
            Orifice K factor  "S, ty 13- X/O
                                                     Meter box number	

                                                     Pretest Y  /,Q/&

                                                     Auditor
                                                                                         AH*
 Orifice
manometer
 reading
   AH
 in H20
     Dry  gas
      meter
     reading
       ft
         Dry gas
          meter
         volume
           V

          ft"
                        Ambient
                        T  /T
                                      Temperatures
Average
  T
Inlet
 T .
  mi
Outlet
  T
   mo
Average
  T
Sampling
  time
    0
   min
                                                                                 ft
                                                                                          .ct
                                                                                                 &
   Y
percent
 error
deviation
 in H20
                 d*'-
                                                                             I
                                                                            /
 I
VD
V


V
- (17.647)(Vn)(Y)(Pbar
                              AH/13. 6)/(T  + 460)
         act - < 1203X0) 
-------
      Date
                                               AUDIT REPORT  SAMPLE METER  BOX
                                                                  Client  (X~
            Barometeric Pressure (Pfa  ,  in  Hg) J?
            Orifice number	
      Orifice K factor
                                                             Meter box number
                                                             Pretest Y	Z
                                                                                    ~"yC
                                                                                     AHa»
                                                                  Auditor XX A! /- fT
Orifice
manometer
reading
AH

in H20

a^6
Dry gas
meter
reading
^ £
ft3
£//, ROO
yfcPV^C/
VB&,d°v
Dry gas
meter
volume
V
m
ft3

/3.V
Tern
Ambient
T /T
* I
°F
(O^ JJV^
C^ / f
0^1 T
Average
T
a
°F

O l\°[^
U '
peratures
Inlet
T .
mi
°F
Sp
o
 mstd = (17'647)(Vm)(Y)(Pbar
 m
  act
              (1203)(0)(K)(Pbar)/(Ta
                                 460)
Percent error = (V
                  m
                   std
                            - V
                               m
                             )(1007.)/(V
                                act
                                       m
)
                                        act
AH® deviation = [(0.0317)(AH)/(Pb  )(T  ^ *60)][(Ta -f 460)(0)/(Vm   )]'
                                                                 act
  ".td
  act
Percent error
AH® deviation
                                           t L
                                            8 .
                                                       ^? . 4 / ^o) =
                                                                                                            f • 'i t
                                    Figure 6-4.  Audit report sample meter box.

-------
             Date
                                          AUDIT REPORT SAMPLE METER BOX

                                                             Client
             Barometerlc Pressure (Pfa  , In Hg)
             Orifice number     #
             Orifice K factor
                                              Meter box number

                                              Pretest Y^

                                              Auditor
                                                                                /~Q
 Orifice
manometer
 reading
   AH
 in H20
     Dry gas
      •eter
     reading
       ft
Dry gas
 •eter
volume
  V
                                        Tern
                         Ambient
                         T  /T
Average
  T
         eratures
Inlet
 T .
  mi
Outlet
                                                        mo
Average
  T
   m
Sampling
  time
    0

   min
                                                                                    m
                                                                     ft
                                                                                     std

                                                                                      3
                                                                                            ft
                                        act

                                         3
   Y
percent
 error
   AH0
deviation
 in H20
                                                                                                                      /-H
        «std - (17.647)(VB|)(Y)(Pbar 4 AH/13.6)/(Tm 4 460)
 "act * <1203H*>/r
 [(/*. ^
                               - (/?-.
                                                                                 •
                                                          ^ - QoJ ][ (^^T . ^_O_
                                           Figure  6-5.  Audit report sample meter box.

-------
      Date
IA
                                          AUDIT REPORT SAMPLE METER BOX
                                                             Client
      Barometeric Pressure (P.  , in Hg)  ^
      Orifice number	
Dry gas
meter
reading
Vvf
ft3
e>^i.oco
8^$l4
Dry gas
meter
volume
V
m
ft3
,
/3.8->T
Tern
Ambient
T /T
*i *f
°F
f*
efl
Average
T
°F

^'•^
peratures
Inlet
T .
mi
°F
• 7s"*> rf^r"""
/ £-*' -^ J
/o£
Outlet
T
mo
°F
/
act
ft3
«./*
Y
percent
error
t.+*
AH®
deviation
in H20
i.ao
 m
  std
  act
        (17'647)((Y)(P
                         bar
        (1203)(0)(K)(Pbar)/(Ta + 460)
Percent error - (V    - V
                  m
std
                          act

                                              460>
                             )(1007.)/
-------
                                              AUDIT REPORT SAMPLE METER BOX
Date
              - 7 -
     BaroBCteric procure ( Pbar, in Hg ) 2 Of,  ~J
     Orifice nuaber	V
Orifice K factor    <," ,
                                    X /c
                                            Client  /-	
                                            Meter box number   /  /^
                                            Pretest Y    / ^ V*^'
                                            Auditor   \] IsJ \
Oritice
manometer
reading
AH
in H20
2./5~


Dry gas
meter
reading
Vi/vf
ft3
5T.2. S"<»

tfiWt
Dry gas
meter
voluM
V
ra_

ID I1-/1")
IJ-,17' /


Temperatures
Tunble'rit
T /T
ai af
°F
e?

& &*
D o
Average
T
a
°F
'•
° rv,.,,
- yv*-
Inlet
Tml
°F
7o

L/ «P-
Outlet
T
mo
°F
*?

jp-'C^— -
(J O
Average
T
in
°F
$7-
rflt
r>
/!• r /


V
ro
act
ft3
t 1 L — S"
/ /. o 6



Percent
error
•+/ 9
•+/• /

U)
  -td
      - ( 17.647  )(  V   )( Y  )(
                                           AH/13.6  )/( Tffl + 460  )
       •ct
               12°3
                                  bar
      \td
       act
     error = ( V
           • ( 17.647
           - ( 1203 )(
                     ~ .(•< o
- V
                         )(  100 )/(  V
                                         5
                                        100
                 •td
                     act
                     act
                                                                                          ff.
                                          Figure  6-7.  Audit report  sample meter  box.

-------
      Dace
             AUDIT REPORT SAMPLE METER BOX
                                Client
      Barometeric Pressure (P.  , in Hg) £-
      Orifice number     V
      Orifice K factor
                                Meter box number	
                                Pretest Y  /, F fr V
                                Auditor   i/ f	
Orifice
manometer
reading
AH

in H20
1 X
'
Dry gas
meter
reading
i f
ft3
37 ?.o 7
V0*.?^
Dry gas
meter
volume
V
m
ft3
q,a^
'
Tern
Ambient
T /T
a . a.
i f
°F
<$#
zy
Average
T

°F
<*"/

peratures
Inlet
T .
mi
°F
f/
?'i
Outlet
T
mo
°F
?LI
#*/
Average
T
m
°F

fr'f

Sampling
time

rain
iv?Y:°-
'^"^'l^

V
mstd

ft3
^
?><-

V
m fc
act

ft3

"V

Y

percent
error
~~ i ^
' **"

AHd
deviation

in H20


 m fc. - (17.647)(V )(Y)(P.   + AH/13. 6)/(T  -f 460)
  std             m      bar              m
Percent error = (V    - V
                  mstd    act
)(1007.)/<-
Percent error - [(_ .	) - (_ •	)](100%)/(_ .	)=__•_
AH@ deviation - [(0.0317)(^ . ^_)/(^l- £ JL J(	• _ _>I
-------
           Date
                                        AUDIT REPORT SAMPLE METER BOX

                                       _             Client   t
Barometeric Pressure

Orifice nuaber
          Orifice K factor
                                     »  in  Hg)  ? "! ~~>Q
O'tr 7
V
"act
ft3
s.,*
Y
percent
error
^ ^7 -/ *>
AH0
deviation
in H20

 I
I-1
U1
std " 
-------
                        THERMOCOUPLE DIGITAL INDICATOR
                      CALIBRATION VERIFICATION DATA SHEET
DATE (e ~ // ~ 6 I   INDICATOR NO. />? £    OPERATOR
N/UJ /7T

TEST POINT
NO.
0
1
2
3
4

MILLIVOLT
SIGNAL*
**
O.OOO
/,S6fr
2*3°
Olv J?
-------
                         THERMOCOUPLE DIGITAL INDICATOR
                      CALIBRATION VERIFICATION DATA SHEET
DATE
INDICATOR NO.
OPERATOR

TEST POINT
NO.
0
1
2
3
4

MILLIVOLT
SIGNAL*
**





EQUIVALENT
TEMPERATURE
°F*
£6;
o~
/0 1
^STo
//>r
i
DIGITAL INDICATOR
TEMPERATURE READING
I 'ftjjijve ; / Tt ^A-o^c'. c-
C / C/ -
V, ^ 6(^
3^ o^
/O^ : /o^
VS7 1 W
\W ; 11^

DIFFERENCE
7.
O 7,
Or/L^
^ / :
"^. .L ,-
o.3'/c
Percent difference must be less than or equal to 1.0 1.

Percent difference:

(Equivalent Temperature °F - Digital Indicator Temperature Reading °F)(1007.)
                        (Equivalent Temperature  R)
Where °R « °F + 460 °F
*  See thermocouple digital indicator calibration verification device calibration
   for these values.

** This point is ambient temperature.  The device is off and therefore is supplying
   no signal other than ambient temperature.
                 Figure  6-11.   Audit  report digital indicator.
                                       6-17

-------
                         THERMOCOUPLE DIGITAL INDICATOR
                      CALIBRATION VERIFICATION DATA SHEET
DATE
INDICATOR NO.
OPERATOR

TEST POINT
NO.
0
1
2
3
4
MILLIVOLT
SIGNAL*
**
o.ooo
/,56k
1.3-30
9$-2°1
EQUIVALENT
TEMPERATURE
V
#3
32.
A? 2-
4^0
//2.-S
DIGITAL INDICATOR
TEMPERATURE READING
°F
g3
30
/oo
±^
II2J*

DIFFERENCE
7.
0
oH\°J»
Q3^%
o,\n
-Q.Ok0^
Percent difference must be less than or equal to 1.0 I.
Percent difference:
(Equivalent Temperature °F - Digital Indicator Temperature Reading °F)(1007.)
                        (Equivalent Temperature  R)
Where °R « °F + 460 °F
*  See thermocouple digital indicator calibration verification device calibration
   for these values.

** This point is ambient temperature.  The device is off and therefore is supplying
   no signal other than ambient temperature.


                  Figure 6-12.   Audit report digital  indicator.
                                      6-18

-------
     Blanks were taken to check the quality of reagents used to



recover and analyze samples.  Analytical results were corrected



to reflect these blank values.



     Lead audit samples were analyzed along with test samples to



insure the validity of results.  Table 6-3 presents the results



of the audit sample analyses, which indicate that analyses were



conducted properly.



     Sampling equipment, reagents, and analytical procedures for



this test series followed and met all necessary guidelines set



forth for accurate test results in Volume III of the Quality



Assurance Handbook.  Therefore, test results reported in this



document should be within the expected accuracies of the method



used.
                               6-19

-------
TABLE 6-3.   AUDIT REPORT  LEAD ANALYSIS
Pb audit
sample No.
1
2
3
True value,
mg Pb
0.800
2.00
2.40
Measured value,
mg Pb
0.782
2.06
2.40
%
recovery
97.8
103.0
100.0
                 6-20

-------
               APPENDIX A




COMPUTER PRINTOUT AND SAMPLE CALCULATIONS
                   A-l

-------
CM
 I

-------
FIELD  DATA







—








SAMPLINB LOCATION NO 2 BARTON OUTLET
SAMPLE t¥Pt LEAD Mi2
OPERATOR J M PRQHASKA
AMBIENT TEMP.(DES.F) 75.
STATIC PRESS. UN. M20) -.40
FILTER NUMBER(S) 0002277
STACK INSIDE. l)irt. (IN) 13. iO .00
PITOT TUBE COEPP. .82
THERM. NO. 129
METER CALIB. FACTOR ,,.4,, 1, 90S
READ 8 RECORD DATA E«*t 11*0 MINUTES
TRAVERSE SAMPLE CLOCK BAS METER VELOCITY ORIFICE PRESSURE
POINT TIME TIME READIN6 HEAD DIFFERENTIAL

DESIRED ACTUAL
1NIT 0 1015 191.000
"' SE01 30*0 1045 ' 225*000 .652 5.10 5.10
> SE02 > 45.0 ,1100 244tf430 »720 5.86 5.86
1 StOd bO.O 1115 £65.050 .720 5.86 5.86
SE03 75.0 1130 289.000 1.140 9.25 8.10
SE03 90.0 1145 314.930 1.200 9.70 9.70
SE04 ''- 120.0 1215 ! 365.000 1,000 8.00 8.00
NE01 135.0 1237 385.000 .720 5.82 5.80
^NtOl "150.0 1252 	 405.000 .660 ' 5.35 5.35
NE02 165.0 1307 427.000 .860 6.90 6.90
NE02 180.0 1322 448.400 .800 6.30 6.30
v ,„.«...,.. ""Htu3.'^» 195*0 ' 1337"?'"W.7*- 472.000 i-*?. 	 " 1{000 ' ' 7.90 T* ""7,90
NE03 210.0 1356 498.550 1.240 9.85 9.85
NE04 225.0 1411 525.000 1,150 9.20 9.20
NE04 240.0' 1426 	 550.774 "1.250 9.96 9,96
TOTALS 240.0 359.774
:"*"™""": • •• - -'- :<-/;:" '**-'-





STACK
TEMP


171.
192.
	 194.
193.
200.
206.
196.
194.
200.
212.
215;
212.
209.
?06;
'Iff.
RUN NUMBER
PROBE LENGTH I TTPE
NOZZLE 5-10ai I.D.
ASSUMED MOISTURE
BAfPLE BUI NUPBEW
METER BOX NUMBER
METER HEAD DIFF,
PROBE HEATER SETTING
HEATER BOX SETTING
'••4
K FACTOR
2BOL-1
5 FOOT
.315
12.0
FB2
1.76
250.
250.
5336.1

OOIRTZ 	



DRY GAS METER PUMP SAMPLE IMPIN6ER
TEMP VACUUM BOX TEMP TEMP
lVE««r) • iiN«.wvK \
INLET OUTLET

94. 84. 5.0
100. 88. 5.0
102. 91; "5.0
103. 92. 6.5
101. 94. 8.0
IV 1 . -f™^jB>- N " '99W *
101. 94. 7.0
94, 99. 5.0
• 94; 90, 5,0
98. 89. 6.0
101. 91. 6.0
'" ' 192. ""-"TfJ. '' ..if'"1
100. 94. 8.0
98. 92. 8.0
98. 92. 8.0



280.
250.
270, '
255,
260.
» jv r't ; '
240.
240.
240.- "
250.
240.
T •-,-.•• '
259.
250.
250; 	
"•Ml"'
EV«FJ . •':*''

T9.
70.
70.
72.
65.
t8. • "•- • • !•• " - •• -y
60.
60.
65.
55.
55.
. ' • - , - - ":"
55.
55.

•i. 	 ' ' - • iVf'*

• — ^t^|r— - - »


-,--. .-•»; . .


i

-------
           PARTICIPATE FIELD DATA • RESULTS TABULATION



PLANT- NAME AND ADDRESS               TEST TEAM LEADER
1 FRESTOLITE MANCHESTER tONA J N PROHA3KA
1 4
. TEST 2BOL-1 NO 2 BARTON OUTLET ;
•
to TE3t UATE
i> TB
11 -i- v:s :• TP
14
TT
II
17 NP
'*«"''•'' •' ' •-jrsV
JO ' X
ON r>
22
., CF
14
t« »
17
" *>
• 0
" VMSTO
34
11
VLC
«•'.••••".•>• •.. • •*.•£*•*
" VNC
40
41
.1 BNO
'.[ ' ' "FMO/^
48
47
F02
41 A : •-• ' ' • • '• •
FCO
Si
•i PNd
ti
MO
»• T* ' ' *" ' • "••••, ••"--'
•« MNS
V:.
ENGLISH UNITS
06/06/61
TIME-START 1015
NET TIME Or TtST, •MIN»;';'iJ 2*0.0
NET SAMPLING POINTS 16
! ^••••V. '^v-|
1.447 8CM
75.5
.101 §CM ' '' ' •"'; r ;
1.05
.989 ' , ''.''"' • ' >• ' ': . • •
.00
20.90
.00 "' "'"" ' ^'^^f^-- •' •••• - ':-^-'W?
79.10 1-..
28.84 ;;
:f " >-*Tl ""'" ' r-^-TT^"^ 	 !" ' ' ""^-

-------
PB BAROMETRIC PRESSURE
PSI STATIC PRES OF STACK
/i*
2
1
4
7
10
It
11
13
t4
IB
17
It
to
|1
»
fT
£•
M
11
32
34
3t
IT
3B
J*
40
41
41
41
44
44
• 7
4t
4*
90
• 1
92
•*
,.
PS STACK PRES, AB8*
28.93 IN-HC 724.66 MM-H6
GAS -.40 IN-H20 -10.16 MM-H20
2B.SO IN-HG 723.91 MH-H6
iS AVtltAtE HIAtK t£MP IVY. F 93* C
VS AV9 STACK 6AS VELOCITY 60.4 FP8 18.4 *P8
AS STACK ARC*
143* 80-IN .092 80-M
OS ACTUAL STACK FLON RATE 216249. ACFM 6123. ACMH
ISO PERCENT I80K1NETIC ^
:'. ,-^i£
MN tdtAL LtA0
M6. EPA 9
}. '..yxn Q4 -•« W?.]?T IWI«li>li«iW l !^BjPpJ.«mP|
PUR TOTAL LEAD
EMISSION #Ate
MN FILTERABLE PART.
I ^ C8 ^l FILTERABLE *ART»
ui PMR FILTERABLE PART.
EMISSION RATE
sS :••-•• ->•• •-• ->f. iff:"* ••• :•»>,.•:•'•••• •"•--' •'/*y?{'my
*• It DEB F, 2 «.92 tN.HC.
'
C?» ,|-*' *3'* '" 9I** ' ''•

^ »034 LB/HR .02 K6/HR
113.3 113.3
..0092 OR/DSCF* 12,016 N6/OSCH
•122 LB/HR .06 KC/HR
•
* "r' 	 '
J

•*•'•" •• -'^jf - ----^-•.' P • •• •';*..'•. .-•: •

f. ' ' . ''"* t , r ™»- '"''' f .'"I- - • ;' ?,^ .,-^- •_, -' >'• . _ K£ ^ ,. T < . ,:•'•' ' "" ' ' T ' ' '
• ' ' -*
11 ../>•'*'



*T -* -.*•-;- 4-" -s-- r 	 " '^ -v 	 ^ ' ' ' * " ' "";l
t\

















-------
               EXAMPLE PARTICIPATE CALCULATIONS TEST  N0.2BOL-1

                    NO 2 BARTON  OUTLET
         VOLUME Of DRt BA8 SAMPLED *T STANDARD CONDITIONS	

         VMSTD * (17.647 • VM  •  T  * (PB » PM / 13.6))  /  (TM * 4*0.)
         VM8TO
                   IT.M7 *    35«.77« * 1.003 •  ( 18,53  » 7.143 / 13.*)
                                                                      333.609 OSCF
                                      »9. »' 460.)
         VOLUME OF HATER VAPOR  AT STANDARD CONDITIONS
V*C «'.104707  •  fLC	

VNC * .04707  *    76. •
                                   3.99 8CF
jwr^r^fr^swj*  ; t, '/\^ "*•'-' *s • ^n^rv>Y rr-^i^, ^f^^fl
                             STACK  4>A8
        BNO  » (100. • VNC) /  (VMSTD * VNC)
                   tos» «
        BMP  m .^•••^•>A«»».
-------
                                                                                                                                      •r
          STACK  GAS VELOCITY AT STACK CONDITIONS

          OELP • SUM,  OF THE 80RT(VH > (TS * 460.))	

          V8  • 85*49 • CP • OELP / (SORT(MW8 * PS)  « PNTS)
          STACK  6A8 VOLUMCTNIC FLON AT STACK CONDITIONS





          OS  *    60.43 *   143. 3600/144 •     216245. ACFH
                                   'L'^C... .1'
                                    AT
          OSSTD  • 17.647 » OS • t>9 * (1. • (BMO/100)) / (TS * 460.)
                    17.64T i    '216245. *  28.50 * (1. • ( 1.05/100))
>0
      >   PERCENT ISOKINETIC
                 (309.5»*( 199.M60.))*((0.002669ft   76,)»(  359.774«1.003ft( 28.53»(   7.243/13.6))/(   95««460«)))
                                             240. *     60.43 *   28.50 *  .315 *  ,315
".         PARTICULATE LOADING •« EPA METHOD 5 (AT STANDARD CONDITIONS)
          PARTICULATE L8S/HR «"• |»A
            R  » CS » OSSTD
          PMR  •     .001 *     1*3315. / (15.43 * 453.6) •
          CS  * 0.001  A UN * l«.«  / ¥MSTO


          C8  i 0.001  * —Si.f « 15;
-------
FIELD  DATA
y


1
11
11
19
14
It
1C
IT
1*
20
21
22
IS
14
21
2<
27
Zi
1*
10
SI
12
13
14
It
37
3B
40
41
42
4>
44
41
*- iiit.niu) iuB«.r>
DESIRED ACTUAL
551.122
591,510 .680 6.70 6.70 211.
614.090 1.100 6.30 6.30 213.
" 636.291 	 '.690 6,70 6.70 209.
657.375 .750 5.70 5.70 202.
676.401 .630 6.30 6.30 204.
•"'•'704,029 "" — 1.360 ' ' 10.30 tv.20 207.
730.396 1.300 9.90 9.90 207.
177.624
7.35 7.34 207.
RUN NUMBER
PROBE LENGTH I TYPE
NOZZLE 5-1041 I.D.
ASSUMED MOISTURE
SAMPLE B0» NUMBER
METER BOX NUMBER
METER HEAD OIFF.
PROBE HEATER SETTING
HEATER BOX SETTING
K FACTOR
-; ' *-, 'WWr^WP^W* • "••• --• "^
2BOL-2
" 5 FT GLASS
.313
2.0
FB2
1.76
250.
250.
9080.4
DRV GAS METER PUMP SAMPLE IMPINGER
TEMP VACUUM BOX TEMP TEMP
(uev.f) iiw*n4Ht
INLET OUTLET

66. 82. 7.0
90. 84. 9.0
84. 82. " 8.0
82. 80. 7.0
84. 80. 8.0
63. "794 -T "tli'B"*
64. 80. 11.0
85. 82. 6.3


260. 66.
260. 74.
2607 " TX).
255. 65.
250. 65.
•901 "" ' '• i*9. . " ' ' lu.'ftjs
250. 65.
256. 68.
.. . f :. .. ... .. .... ..,„. -$»<>,-, ,-...,.,, . , , ,f . ,

'"""""•• ' '=; ^^^'^.J^f^^^-- :'-^ •"—' 	 •• '.* -^ -----r-. • - -iw
f
....... ;,,..«,,;,,,r,r^:,p, , ,v ,r. . .. ...... ..... ...,., ,,^ff^,,v ,_ 	 ..,.,..,

* - •'•••.'•'
- *-'•
i . *'^ • i-'-f,"* ' ' ' ••'".- "*

,.,,,,„ ...p


















'

-------
           PARTICIPATE FIELD DATA • RESULTS TABULATION



PLANT- NAME AND ADDRESS               TEST TEAM LEADER
f\ i- .;"
t PRESTOLITE
MANCHESTER IOHA PROHA8K A/THOMAS
. TEST 2BOL-2 NO 2 BARTON OXIDE OUTLET
7 "
I
I. TEST OAT£
<» TB
11 ' T TF !*»•.„,<*•••
14
TT
It
17 NP
It
10
», DN
22
» CP
• 4
Zt ,' ,
It
10
if '• •• ,- TW : ^v*c-fl^-
," VM8TD
34
" VLC
37 '-{'
39
VNC
40
41
BNO
', FMO
4«
«4 PCO*?
47
.. P02
PCO
St
9> r rlC
It MD
• • MMS
v
,-(:,^,k- ; ;
TIME-START
NET tIME OP TE8Y, MM^/jS^f
NET 8AMPLIN6 POINTS
1H ili^ AWWfWSBT'WHPWBpB^pPPJp
SAMPLIN6 NOZZLE DIAMETER '
PITOT TUBE COEFFICIENT
DROP
vOLuni 0^ OwV CAS SAWPiED
AT METER CONDITIONS
VOLUME OF DRY 6AS SAMPLED
AT STANDARD CONOillONS"
TOTAL H20 COLLECTED IN
1 MP1 NBER8 •• IHW BIL 1C M - BEW W f ' l'"
VOLUME OF MATER VAPOR
AT STANDARD CONDITIONS"
PERCENT MOISTURE BY VOLUME
MOLE^ FRACTION DRY 6AS
PERCENT C02 BY VOL.* 'DRY
PERCENT 02 BY VOL.» DRY
PERCENT CO BY VOL.. DRY
PEttCCMt N2 BY VOX*. OHY
MOLECULAR NT-DRY STACK BA8
MOLECULAR NT-8TACK BA8
EN6LI8M UNIT8 METRIC UNITS
06708/81 06/08/01
1545 1549
IB**--'- ••' '•* "" '**:''> • IBCI '• • '- •' ' •' 	 	 • • ' f,
120.0 120.0
8 8
.313 IN 8.0 MM
.82 .82
.'•'HWM IP*H2U '•" \ !••»« »«W»««O • *^<'*™ " :" '" ."• ' •- i i ST)
ltt.824 CU-FT 	 5.035 CU*M
168.192 SCF 4.762 8CM
4T.7 47.7
-,— -7--.' •-?- "-' "™- •«^ln^ "' ' "I '-'-•.' n HljTT. i, ,n ... ;?,..j . .... im—^n -^ '" ' "'^'-.'JS'
2.245 SCF .064 8CM
1.32 1.32
.987 .987
,xn> .00
20.90 20.90
.00 .00 . l?
f^.jO 79.10
28.84 28.64
18.69 28.69


10
1 Z
(4
IB
1
2
2
t
t
1
t
2
2
2
t
f
3
*
*
X
1
4
47
41
SO
5 t
91
91
• 4
Bt
94
4*
«O
«t
44
*•
17
• t
• 9
7
7
7
y

-------
PB BAROMETRIC PRESSURE 28.48 IN-HG
PSI STATIC PRES OF STACK GAS ».40 IN-H20
(i :-••"• - " . • 	
, :> PS STACK PRES, ABS. 28.45 IN-HG
a
, T3 AVERAGE STACK TEMP 207." F
! VS AVG STACK GAS VELOCITY 61.9 FPS
i AS STACK AREA 143. SO-IN
i. HSSti) STACK FLOM RATE, DRV" 164536. 3CFH
!, OS ACTUAL STACK FLON RATE 221508. ACFH
ISO PERCENT ISOKINETIC _ 95.1
.. MN 	 TOTAL LEAD '"""*"" 47.3
i, . MG. EPA 3
" PMR TOTAL LEAD .102 LB/HR
12 EMISSION HATE
" MN FILTERABLE PART. 70.0
" ,„ CB FILTERABLE PART* ' .0064 6R/DSCF*
". M PMR FILTERABLE PART. .151 LB/HR
,. ° EMISSION RATE
], * 68 OEB Ff Z*.»i IN.HG.
1*
» '•'."' "••'* ' ' ";' '-,""1." \ '
40
41 / '
4S .,,P*> ;«,-'.»*- •• r , •• t -. ,*-.,-• -'*.. .-.*?m-$™\-^f -%-^i$$';-m"^Kj$ • •* ' '.' •• • '•* %'-. -T • '^ - • . l-( ' • "*;
.. ' '• '• •;:-;>:• 'r -4:. :••'• '
45
4« k
47
4«
SO -;
B»
91
• I
B4
;:;
723.39 MM-H6
-10.16 MM-H20
722.65 NM-HG '
18.9 *PS
.092 SO-M
4659. SCWH
6272. ACMH
• • >
47.3
.05 K6/HR
70.0
14.702 MG/DSCM
.07 KG/HR
"*',-r • '

... ,,.... tf ,,„,,,,,., . . . . ^


.
• :^,-T>!f, • , ,























-------
            EXAMPLE PARTICIPATE CALCULATIONS  TEST  N0.2BOL-2
                 NO 2 BARTON OXIDE  OUTLET
—	VOLUME OP DRT CAS SAMPLED  AT  STANDARD  CONDITIONS	
      VMSTD * (17.647 * VM *  Y *  (PB  +  PM  /  13.6))  / (TM » 460.)
           17.647 *   iff.824 •  1,003  *  (  26.46 * 7.338 / 13.6)
 VM8TO • •«*«»*»•»***»••«•••-—•-•••»«•"—-«—--—-—•----•---- i
                                   ~»6~U77"
                                                                          168.192 DSCF
                                   feJ.
      VOLUME OF HATER VAPOR AT STANDARD  CONDITIONS
      VMC   .v4rvr *  LC
      VMC • .047*7 *   40. ft   2.23  SCF
                                                           w"*p-'
     'PERCENT notSTORE in StAcR  B*a\
      8MO • (100, * VNC) /  (VM8TO  *  VNC)
...,
*r
           100. •   2«t)
       ^~^-«^^—.	*	>^^M.^~.	.^   A  ««  AJFDftffliY
       ^w^w•«•»»»»«w»™»ww»^»»w»ww ••   1t*m  rfcWWCRI
      MOLE FRACTION Of Out itACK
      PMO * (100. • 0wO)/  100.
      AVERAGE MOLECULAR NEtOMT  OP  DRY  STACK GAS
 MO * (PC02 * ,44) *  (P02 *  ,12)  •  (PNt * PCO)  * .28
~	T—.TOM4/100)  »  (|0.9«32/100)  »  ((79.1*  tt~*-t9TtWnr~~287^4^
      MD
      MOLECULAR HEIGHT OF STACK  GAS
  h
      Mli3 T~MTTTi~Tl. """TBHO/lOO))  *  18.  • (bwu/1001
      MNS •  28.84* tl. -(  1.32/100))  *  18.  • ( 1.32/100) •   28.69

-------
          STACK GAS VELOCITY  AT STACK CONDITIONS
                                                                                                                                                   t
          DELP • SUM. OF  THE  80RT(VH * (T8 * 460.))	
/{|p " ,<  '	'	'	•	•.-•••---	'	'"*T*	'	"—'      '"•  •' '•-: '•    '    :r •'•	      """"'  '• ••'•''-•  "~"• ;;•• •. •: <•"•. "-rv"   ••- -        •,•  ••-••-•••^\ i\
 , '        VS « 89.49 * CP  * OELP / (SORttMNS * P8) * PNT8)

          vS * 69.49 •  .82 'K  201.832 / (SAKT( 28.69  •  2B.43)  •  "~9* *   6l»90


         —, ,, ,,,.,,,   i   ,,,„ ,v —T	••:•""; •	.""'"—'—^-—'—'—        • r

          STACK CAS VOLUMETRIC PLOW AT STACK CONDITIONS
          aa • vs « »s^

          OS •   61.90  *    143.  3600/144 •     221908.  ACFH
,.  —-*	8UCR 6*3 VULUMtTHIC  FLUR *l iUlBANU LUNDH1UN8	

          OSSTD * 17.647  *  OS * PS • (1. - (BNO/100))  /  (TS  + 460.)
ia

XI

14
                            »  ?;?  221308. *  28.43 «  (t.  •  t  1.32/100))
          QSSTD •....^.^•••••••..........»...........—........... •     164938.  SCPH
)»
          MRCIJIT ISOKINETIC
„   M'   |Sit * (543.58*(184460.J)»C(O.OOi66*"VLC)#{VH«Ti
»
                 (303.98*(  207.»460.))*C (0.002669*    *•«)*<   *^'a2^*^'^^*5 g*'***f	7.338/13.6) )/(  83.»460.)))

                               ;               120. *      61.90 *   28.49 *  .313 *   .313              ^
          PARTICIPATE COADINC  •• EPA METHOD 9  (AT STANDARD  CONDITIONS)
          OS * 0.001 * MN *  1»#*J / VM8TD
                          */.J • 13.43 /16d.i92 *.T04  fcR/Oacf
          PARTICULATE L0»/N«  •- EPA METHOD 9       '
                                     ^'433.6)

          PMR •     .004  •      164938. / (13*43 * 433.6)  »       .10

-------
FIELD  DATA
> SAMPLING LOCATIO* NO. 2 BARTON OXIDE OUT
« SAMPLE TYPE 	 " 	 "LEAD M12
• OPERATOR J. N. PROHA8KA
. AMBIENT TEMP.COE8.F) 70.
, "in!fW,""'" "".' BAR. PRESS. (IN^HCI " W3 •• " IB. 60 ""•'""••"' 	 	 .••" " '
. STATIC PRESS. (IN. H20) -.40
. FILTER NUMBER (s) 0002273
10 STACK INSIDE DlM.tlN) 13.50 .00
PITOT TUBE COEFF. .80
11 THERM. NO. 128
!!' ' ' METER CALIB. FACTOR « " :^.U003
.. ( READ • RECORD DATA ItBRt 15.0 MINUTES
.' . TRAVERSE SAMPLE CLOCK SAS METER VELOCITY ORIFICE PRESSURE STACK
t. POINT TIME TIME READING HEAD DIFFERENTIAL TEPP

DESIRED ACTUAL
» INIT 0 1433 899.803
,. SE-2 30.0 1503 i ' 935.000 ,7«0 .40 .40 214.
„ 9E-3 45.0 1518 959.800 1*130 .40 .40 211.
,. '"{pi SE-4 " 60.0 1533 976.000 1.200 .90" .90 215.
,. 1 NE-1 75.0 1552 3.550 . .640 .00 .00 187.
» J"j NE-2 90.0 1607 25.700 .900 .80 .80 204.
NE-4 120.8 1637 73,009 1.090 7.90 7.90 208.
TOTALS' 120.0 ' 173.206
AVERAGE 6.79 6.79 206.
I

,,,,,,, ,,„, .,„_,.

" ; ' ''*"" " ""^FtST"' " "
•V
''" '
,'• -' 'DATE
RUN NUMBER
PRDBE LENGTH > TYPE
NOZZLE 5-1041 I.D.
ASSUMED MOISTURE
SAMPLE BOX NUMBER
METER BOX NUMBER
PETER HEAD OIFF.
PROBE NEATER SETTING
HEATER BOX SETTING
K FACTOR
DRY GAS METER PUMP
TEMP VACUUM B
IDCH.f) lin.HV} 1
INLET OUTLET

74. 65. 7.0
82. 70. 11.0
83. " 73. 14.0
78. 74. 6.0
79. 74. 9.0
85. 75. 18.0
78. 71. 9.1


f " — , '3,'."

" ^


280L-3
5 FT CLASS
.313
2.0
FB2
1.76
250.
250.
49809.0
SAMPLE IMPIN6ER
OX TEMP TEMP
frev.rj (bcv.p) • - - •*•


250. 60.
300. 60.
300. 60.
300. 70.
300. 70.
'9^ W« ' T"
0. 0.
222. 48.
• V-' "f

,






0
1
X
-\
4
•
7
ff
0
t
a
i
4
9
28
90
11
It
1
1
1
1
18
40
4
4
t
4
4
0
I
1
4
t
0
I
«S

7t
71
-'

-------
           PARTICIPATE FIELD DATA • RESULTS TABULATION



PLANT- NAME AND ADDRESS               TEST TEAM LEADER
1 PRESTOLITE MANCHESTER IONA ' J.
'. TEST

t. TEST
TB
',', TT
" NP
10
., ON
tt
» CP
14
» " ','•-"• '"•"'""fH*"^^'
tl •
17
,. >
" VMSTO
14
SB
VLC
SB
VNC
10
41
., BNO
«, ?F~.--.-i>
FMO
4B
4< Ptoi
1 P02
PCO
1
PN2
MD
B • "k '
MMS
2BOL-3 NO. 2 BARTON OXIDE OUT
' ' '•'• •••»*; -;•,:• ' •'!•;,' ;.£•;. ','' ..' . -' !
DATE
TIME-START
NET TIME OF TIST, fltll*L 1%
NET SAMPLIN6 POINTS
SAMPLING NOZZLE DIAMETER
PITOT TUBE COEFFICIENT
DROP ; ;
vuLunt u^ iittV HAS aAn^Lcb
AT METER CONDITIONS
VOLUME OF DRY 6 AS SAMPLED
AT JJTAwunitu CUnUillONS*
TOTAL H20 COLLECTED IN
inPlNUtRB UNW 91I.1CA VtLWk*« ••
VOLUME OF' HATER VAPOR
PERCENT MOISTURE BY VOLUME
MOLE FRACTION DMT 6 AS
ctKCcnt £02 BY vuu«» DMr
PERCENT 02 BY VOL.* DRV
PERCENT CO BY VOL. » DRY
PERCENT N2 BY VOL., DRY
MOLECULAR NT-DRY STACK 6AS
MOLECULAR NT-STACK «A8
N. PROHASKA '

ENGLISH UNITS
Ofc/u^/oi
1433
120.0
8
.313 IN
.80

166.826 SCF
48.8
2.297 SCF
1.36
• 986
.00
20.90
.00
79.10
28.84
28.69
t.x:v ' ;'- '"-' " • '•'<

METRIC UNITS
1433
120.0 >2i';Mftj-i.
8
8.0 MM
.80
MK-.~.'iW»8 WMV1IU •••.. • ".-•-i.^i'if^..f^tvv^-n^-n. ^•••: •• •••-. •• - ,] J-!!fH!||^|
^.'ioS CU-M ' 	 	
• **•' ' ' T -*'••••-- ^« ^^JS^^WPW1 	 V-:; •' *•• -) - ...iO
28.64
28. 6«
K
















V

-------
       PB

       PS I
BAROMETRIC PRESSURE

STATIC PRES OF STACK GAS
                                           28.60  IN-H6

                                            •.40  IM-H20
                                                               726.44  MM-HO

                                                               -10.16  MM-H20
      PS
STACK PRE8, ABS.
                                           28.97  IN-HB
              ..Jr..
      vs
                         STACK  tcW
AVS STACK 6AS VELOCITY
                                          go*.

                                           98.2
rrs
                                                               729.64  MM-Mfi

                                                              -IT;	"x 	—•

                                                                17.7   KPS
                 STACK  AREA
                                10.

                            "IS9512T"
                                                 SO-IN
Q33TD     STACK FLOW KATE* OUT*

OS        ACTUAL STACK FLOM RATE       208240.
                                                        3CFH

                                                        ACfH
                                                                  «092 SO*M

                                                             "4*Q*.8CWH

                                                              98f7.    ACMH
                                                      M.S
                 PERCENT  I80KINETIC
      MN
            EMISSION

          FILTERABLE PART.
                                 45.9
                                                                	,07  KB/MR


                                                                43.9
 . *-.«5r
  ->--
    I
C8
                 FILTERABLE  PART*
      PMR
   ui
          FILTERABLE PART,
            EMISSION
                                         0K/DSCF*

                                   .089   LB/HR
                                                                 9.20« M6/D8CH

                                                                   .04  K6/NR
11
n

-------
                EXAMPLE PARTICULATE  CALCULATIONS TEST N0.2BOL-3

                     NO.2 BARTON  OXIDE  OUT
          VOLUME OP DRT 6*5 SAMPLED  AT  STANDARD  CORDTTTOW
          VMSTO • (17.647 * VM  *  Y  •  (PB * PM / 13.6))  / (TM * 460.)
                    17.647 •    173*206  *  1.003 * (  26.60 * 6.788 / 13.6)
          VMSTO » ........—..•.»*.—..—••..—..——..—.—•««..... •	166.826 D8CF
         	C	75.  *  460.)	™
         ^                    i.;  >     .•'•••'  '   •    . i
          VOLUME OF NATER VAPOR  At  STANDARD CONDITION*
          VMC « .04707 * VLC	   —"—"	"

          VMC « .04707 *   49. •    2.30  SCF
                           IN 3TACK


          BMO • (100. * VNC) /  (VMSTD  *  VNC)
                    100. •   2.30
                    «•.•»»...•—.»--»••»»•  •   1.36
                             f2.30
          MOLE FRACTION OF DRY STACK


          FMD «~Cl6u« - BHO) / 100.~


                    100. -	1.4
                         IMW1

                         100.
i«j	    AVERAGE MOLECULAR NEI6HT OF DRY  STACK  GAS
Si 	
          MD • (PC02 * .44) *  (P02 *  .32)  *  (PN2  •»  FCO)  *  .20

         " MO »"t  iOO»44/lOO)~»  (20.9*32/100")  »  (C79jn"»~.07""T"" 28/100 »
          MOLECULAR HEIGHT OF STACK 6AS

          MtoS *~MD"TT C1. • (bWu/100)) T  18.  *

          MNS *  28.84* (1. -(  1.36/100))  »  18.  *  (  1.36/100)  •   28.69

-------
STACK GAS VELOCITY AT  STACK CONDITIONS



DELP « SUM. OP THE 30RUVH *  (TS  *'460.))
' VS » 89.49 * CP * DCLP / (SORT(M*8 * PS) * PNTS) •
4

STACK 8AS VOLUMETRIC
1V4.090 / 19UNTI ZB.69 * 2B.37J * 6* * 3C.11 FP9 •
7
0
PLDN AT STACK CONDITIONS \°,
12
OS • VS * AS * 3600/144 "
14
OS • 98.19 * 143. 3600/144 • 208240. ACPH ','.

st*CK BAS VoLUHetttJt
OSSTD « 17.64? * QS
17.647 i*

I
PEftfctKT I80KINETIC
ft* Y*d J "lift* 4A4/V4 JiJL.
-J (309. 96* ( 206

PARTICIPATE LOADIN6
, 1 •
-*' "i ', t;'? "' " ; **
"**" Ha' if "% "' 'iri ' ri iu4 	 ~ ' '"" • ' "
22
•PS * (1. - (BNO/100)) / (TS * 460.) "
208240. * 28.97 *(!.-( 1.36/100))

206. * 460. J "" »
10
It
>t
^_^;,,,^, ,,,,. ., . .. , . -. ,. . . .. ^
0.) J«((0.002669*VLC)*(VI"l*T*lP8»(PH/13.b))/(TH+460.)))/ (TT»V8»P8*DN«DN) ,,
.4460. ))*((0, 002669* 49.)*( 173. 206*1. 003*( 28.604( 6.788/13.6) )/( 79.»460.))) \'a
120. * 98.19 • 28.97 * .313 » .313 ;;
.44
45
i 4«
— CPA METHOD 9 (AT STANDARD CONDITIONS) "t
CS • 0,001 * MN • 19.43 / VM8TO 1°
92
ca • tf.Ooi * 74.0
PARTICIPATE L88/MR »
Pnft « CS * ASSTO / I
PMR • .00? *
• 13.43 f 166.0(£b * .UUf 6N/D9CF •>
• 4
•^tP* MtTHOD .9 ;;
• 0
199962. / (19.43 * 493.6) • .19 "
•>• • : .';''•;' • "' ~W' •* ; '. •' ; ' V '•",'''' "' • ••
- *- C7
• •
70
72
L 	 _ ._._ .. _ 	
7*
3

-------

(t

















F - 	 ' ' ,, ^Wv;. - -:,j
' PLANT
I SAMPLING LOCATION
SAMPLE TYPE
„ OPERATOR _ _
AMBIENT TEMP. (OEG.F)
BAR. PRESS. (IN. HG)
i STATIC PRESS. (IN. H20)
FILTER NUMBER(S)
STACK INSIDE DIM. (IN)
PITOT TUBE COEFF.
';. •'•'.- ;" " •' THERM. NO.
LEAKAGE
METER CALIB. FACTOR '

FIELD DATA
* PRESTOLITE»MANCHESTER
N0,l BARTON OXIDE OUTLET
PARTICULATE
PROHASKA
70.
28.60
-.70
0002130
13.50 .00
.82
.000 CFM • 3
1.044
READ » RECORD DATA EVERY 15.0 MINUTES
TRAVERSE SAMPLE CLOCK GAS METER VELOCITY
".: ' ::Y..'^-'V poiNT • • TIME '' TIME Ji^
NO. (MIN.) (24-HR
CLOCK)

HEADING HEAD
(CU.FT«) (IN.H20)




.0 IN.HG
ORIFICE PRESSURf STACK
DIFFERENTIAL TEMP
(IN.H20) (DEG.F)
DESIRED ACTUAL

DATE
HUN NUMBER
PROBE LENGTH ft TYPE
NOZZLE ! I.D.
" ASSUMED MOISTURE
SAMPLE BOX NUMBER
METER BOX NUMBER

06/09/81
1BOP-1
5 FOOT GLASS
.251
2.0
113
F10
METER HEAD D1FF. 1.80
PROBE HEATER SETTING 80.
MEATtR BOX SETTING
K FACTOR
DRY GAS METER PUMP
(OEG.F) (IN.HG)
INLET OUTLET
«50.
2198.0
SAMPLE IMPINGER
•Ol fEW» TEMP r f '• • '
(DEG.F) (OEG.F)


£'rm.>"?r*v- INIT f •-•• o •'•-'• mo -••**'
SE-l 15.0 1545
*?•: . 3E-2 SO.O 1600
^ SE-3 45.0 1615
00 SE-4 60.0 1630
NE-1 67.0 1652
<: •••."? ^hsY' ' NE-l • ' 75.0 " 1700 ',V-- '
NE-2 90.0 1715
NE*3 105.0 1730
NE-4 120.0 1745
TOTALS 120.0
AVERAGE ' ' • -•• -• "*;'•;' • ' '!

\> •-/;.•:- '•••.; •-:..-.,'_-' 9 ' •' ." , .-, ' * ^ *** • "'^i- ' •' -
902.886 7
915.000 .640
927,450 _ ._*780_
942.000 1.050
957.316 1.000
962.000 .560
969.7SO '•' .BOO
984.000 .970
999.130 1.050
14.052 1.000
111.224


1~ ""• -fT '' ' '~ r'-~ ' ' -.'&'*"•,*':'" -.•"•'
2.10 2.10 197.
2.50 2^50 207.
3.40 3.40 215.
3.30 3.30 208.
1.85 1.85 208,
ifr 8.60 2.60 " 209. r1"
3.10 3.10 216.
3.40 3,40 21«,
3.30 3.30 213.
,,_,, 2^«i > 2.0* 810.


68. 68. 2.0
74. 68. 2.0
82. 72. 2.0
87. 75. 2.0
85. 78. 1.0
83. ' >••' 78. T '^•'«4-»"'
86. 78. 2.0
89. 80. 2,0
92. 82. 2.0
• -•:. «'*^w

.»..'.- .. V. - •.*,**--. **,
325. 46.
300. 50.
270. 52.
250. 56.
220. 52.
*••'••' nO. • *- 53. " f j-v ••- •
260. 53.
240. 54.
2bO. 62.
^TT •; jjt .T . -.rt.. •

^ ?1^-*?? lis--!'-". • 'f.- \£ ;.*• ' ' ' . ,+s . ^ .7
V









-WI£J**v- - • • - ^-f

» . '
^

o
-j
tn
t i
IP
I
"i
'•;
11
J7
11
1 *
4 4,
«7
49
•> 1
? ^
• *
r
i
j
4
«•
• t
7O
T 1
:;

-------
PARTICIPATE FIELD DATA t RESULTS TABULATION
t jrh--: -'PLANT* NAKE AND AOOffEST *" • • ' '• •"'
PRE8TOLITE, MANCHESTER
TEST TEAK LEADER
PROHASKA
TEST 1BOP-1 NO.l BARTON OXIDE OUTLET
!• »,.'.,.,
f
TEST DATE

'•*" ' TB T1NE»START r 	 p- - -.^ - •
TP TIME-FINISH : &..
" ' • jL.'ii •
<• TT NET TIME OF TEST, MIN. ,
%J
» NP NET SAMPLING POINTS
T METER CALIBRATION FACTOR
Z1 .
< ON SAMPLING NOfZLE DIAMETER
1
« CP PITOT TUBE COEFFICIENT
PM AVERA6E ORIFICE PRESSURE
'j DROP ;
B
• > VM VOLUME OF DRT CAS SAMPLED
^ AT METER CONDITIONS
TM AVERAGE CAS METER TEMP
• VMSTD VOLUME OF ~0~*T~CAS "SAMPLED" "
* AT STANDARD CONDITIONS*
• . *
T "' Vltf**- *?r 'TOTAL H*»"MtitWTtO W ' ** ",
IMPINBERS AND SILICA GEL, ML.
3 '.
VNC VOLUME OF MATER VAPOR
AT STANDARD CONDITIONS*
X
'^ " MKI « PERCENT MOI8TVN1 IT VOLUME
•1 ,
FMO MOLE FRACTION DRT GAS
A
' PC02 PERCENT C02 BT VOL.» DRY
•
•'^""•" Pbk "**'• PEMCMt Of IV>r-'f8t*7"WV T*.?*''1
» ' « ' '
^ 	 _.pQO. 	 PERCENT. CO..BT, VO.t, »_._DR.T 	
2
>. PN2 PERCENT N2 BT VOL., DRT
4
Mb MoLtiEOLAll t»Ti.(JiV STACK 4AS
c
' MNS MOLECULAR XT-STACK GAS
ENGLISH UNITS
06/09/81
ISJfli
1745
120.0
1.044
.251 IN
.82
2.84 IN-H20
111.224 CU-FT
ff.f F ' ' '
109.489 SC~F
*
2.024 8CF
• 1,82 •^f—^- .
.982
.00
" 99*19 •-,;-••,— - •
79.10
18.14 ' '
28.64
r
L
3
4
7
-I
METRIC UNITS [!»|
06/09/81 "
iSj6 - - -w - - -
1745 ;;
.»•>,
120.0
tl
9 ri
»••«« !"!
• 2 n
6.4 MM
11
.82 !i
72.1 MM-M20 :;;
'••«]
"1
5.150 CU-M "
v , «•>(
26.2 C t '
4
T.foo'sctii 	 	 " " "'
4
4

.057 SCM
B«
f .82 -•-.•• "- -«' r •*•?• • ' i» • ' i
.982 U
.00 :;
• 4
• 00 84
<"
79.10 "
Tt
18.84 ;
28.64

-------
                                                                                                                                     , (-1
                                                                                                                                      [,
PB
BAROMETRIC PRESSURE
                                            28.60  IN-HG
726.44  MM-HG
*£•".- PS I •>•,
PS
TS
VS
1 Q8STD
• *->;?••? as
t
1 ^ ISO
1
" MN
11
it •-r;"'; '
CS
11
" PMR
Z
'
2 1
' bJ :•
* o CS
2
PMR
i 7 •••• '. '•'
»
MN
4
I
" C3
PMR
40
MN
4t
CS
'9
" PMR
7
S
•" ' MN
0
1
CS
91
• 4 PMR
si
31
V *
	 STATirPlEB dF'SfACVSAS1 ''•"
STACK PRESr ASS.
AVERAGE STACK TEMP
AV6 STACK GAS VELOCITY -
STACK AREA
STACK FLOW RATE* DRY*
-' ACtUAC if *CK FXOII **ft "?
FILTERABLE PART
MG. EPA 3
FILTERABLE PART
FILTERABLE PART
EMISSION RATE
MG! EPA 3
COND. INORGANIC
CONO. INORGANIC
EMISSION rUTf:'' •*' ''V^' '
CONO. ORGANIC
MG. EPA 5
CONO, ORGANIC
COND. ORGANIC
EMISSION RATE
TOTAL PARTICULATE
MG. EPA 5
TOTAL PARTICULATE
TOTAL PARTICULATE
EMISSION RATE
FILTERABLE LEAD v ••?>?•••" ' •'•'"
MG. EPA 3
FILTERABLE LEAD
FILTERABLE LEAD
EMISSION RATE
66 OEG F, 29,92 IN.H6.
•.70 IN-H20
28.33 IN-HG
210. F
39.0 PPS
143. SO-IN
155822. SCFH
210994. ttPM '
101.6
32.5
.0046 SR/D8CP*
.102 LB/HR
•,fl*T •' •••>•
.0002 GR/DSCF*
.005 LB/HR
T,7.
.0011 6R/OSCF*
,024 LB/HR
41.9
,0039 8R/D8CF*
.131 LB/HR
IT.9
.0023 GR/OSCF*
.056 LB/HR

* 1 1 + f O Wff ™ f V *' ' • • ' i
723.13 HM.H6
99. c ;
16.0 «PS ' ;i ~ • ' "" -' '
4412. SCMH ','.
3f7t. ' *CWM ' ••' ' * ! ** '"••;" •• •••'"•'•' 7?~':
_.. . , '
ioi.fr .-... . "• „;• •, ','
32.5 "
10.484 ^6/09CI»
. ....
.05 KG/HR ^'
i
.546 H6/OSCH "
,00 KG/HR
"*'r'
2.464 M6/D8CM »
,'. ., - . v -• •. -,: S ' '"I'. '•','. ' • 4»|
.01 KG/HR
411 •< !.'
"r"i
13.916 KG/D8CM '."
.06 KG/HR "|
"i
; 17. f ^ . .f • ..- • :••..- ---r.iy. .5-. v :.••• --, ' -• -"
3.774 MG/D3C*
.03 KG/HR
j

-------
                 EXAMPLE PARTICIPATE CALCULATIONS TEST N0.1BOP-1
fi,¥~'""-r '""  ''•'"•'        MO.l BARTON OXIDE OUTLET
           VOLUME OF DRY GAS SAMPLED AT STANDARD CONDITIONS

          "VMST0 • (17.»47 • VM • Y * CPB * PM / 1175)1 V  IfM k
14
                     100. •   2,02
     i   ~TSib • .—i-i—.«ii.......:.-.'i^nt  t;i2~pfRCENf
    to               109.489 »    2.02
                                                                                                                                                •'e
»|          MOLE FRACTION OF_DRY STACK 6A3_
34J
           FMO • (100. - BMO) / 100.
                     10V*•••

                          100.
.'         FMO • .••...•*...•*••.•..*•*• *   .982
                                                                                                                                                 c
    T^     AVERABE MOLECUUAR NKIVMT OF OUT STACK BAB
                                                                                                                                                 i ^
««
           MD • (PC02 * .44) » (P02 « «32) »  (PN2 •» PCO)  *  .28

           MD « C  .00*44/100) * (20.9*32/100) * ((79.1*  .0)  *  28/100 »   28.84
                                                                                                                                                 C
                                                                                                                                               t

                                                                                                                                                 €
  sr
• 1
          .Mpl-ECUL»R_l»fIOMT OF  STACK; JBAS

          MNS • MD • (1. - (BNO/100))  *  18.  •  (BNO/100)
                                                                                                                                                 C
        '  Hni i  H«M*'f |«'*( lit^/ICOr »'li, •  I  i.eg/tftO)  i   II. *<
                                                                                  *•
                                                                                                                                                7«

-------
   STACK 6A3 VELOCITY  AT  STACK CONDITIONS
   OELP « SUM. OF THE  SQRT(VH * (TS * 460.))            ,



   VS • 85.49 *  .82 *  216.410 / (30RTC 28.64 * 28.55)   *    9.  >   58.95 FPS



	STACK. 6A3.VOLyMeTRIC_Fl.Q>LAT_STACK. CONDITIONS	 	   -		      			

   OS • VS * AS * 3600/144

   OaTi58~.95 *   143V 3600/144 •   ;210954, ACFM      !       ''  '               ""'    ~~~~'  f^~~:          !

	      ...	.	.	;	._	  	,	i .  :		 _._	.	_J	*"J

   STACK CAS VOLUMETRIC  FLON AT STANDARD CONDITIONS

""""OSSTD * 17.MT « 08 * PS * (1* * (llSo/ToT)) f ttl 4 460.T~   ~r~~~    '—       r^r"~    -w^wf^-T^ f  / 'T  ':'        "

_	ir.MZ_*	«lo«lft*_*_J»*s.s_t__O..j_.r_<  1,82'ippj)	    _	
   08STO * ————————.—————————— •     155822. SCFH
                       (  210. * 460.)



L^HCEJLUWRIMCTJC
                                                                                                                                           ' ^
J  ISO • (305.58*(TS*460.))*((0.002669*VLC)*(VM*r«(PB*(PM/13.6))/(TM«460.)))/(TT*VS*P3*ON«ON)                                            {C

"   '~~'    (305.58«( I10*«460.))*( (0.002669*'  4T.TR   fll »224«1 »044*( 28.60«(    2.819^1 Ji*JIW1 'ft»l
   ISO •--.-..--*•*•--•---•*••*•----.•---•-•-••--•-•----"---•----—————"—————•«*—•—"—  « 101.63 PERCENT             C
	120. *	58.95 *	28.55 *  ,25t •_ .251	   	



   PARTICULATE LOA01N0 •• EPA METHOD .5 (AT ITANOARO CONOlttONS)    '     ~~T  '       '"'•  ^^""[^ ;^*«s%^5-^'"^    * '^' ' :'-r:"' •'•'' ~- •:" '*>'

   CS « 0.001 * MN « 15.43 / VM3TD	,	;	.  .  .  .. .	,	

   CS » 0.001 *    32.5  * 15.43 /   109.489 •     .005 6R/D8CF                                                                          "\ C


                                                                                                                                           !(.;
   PARTICULATE LB3/HR  •• EPA MfTHOD 5

   PMR « CS * OSSTO /  (15.43 * 453.6)                                                                                                      C

   PMM *  !   .005 *      115812. / (15.43 * 453.6) *     '  iTf   "   '     :  •    ;;-      S" '"""''  ?• :«P%f VT/ H"*'^" '  .^"'••^r> "*T"             .  .
                                                                                                                                            C


                                                                                                                                            t

                                  "f';;•.;:     7~~~          :   ~~*~~    .•;  :' T" "' , -•;• -.   ~ : •-•WT--T-:-  ~ ^j'.*, ~ •
                                                                                                                                            v.

-------
FIELD  DATA
> SAMPLING LOCATION ENTOLETER SCRUB
' 	 	 SAMPLE TTPE "" ' LEAD M12
. OPERATOR PROHA8KA
. AMBIENT TEMP. (DEC. F) 15.
i STATIC PRESS. (IN. HIO) -Iso
FILTER NUMBER (8) 0002289
OUT





,» 	 STACK INSIDE DIM. (IN) 24.75 ".00
PITOT TUBE COEFF. .80
THERM. NO. 128
','. METER CALia. FACtOR K044
READ t RECORD DATA EVERT IS.O MINUTES
TRAVERSE SAMPLE CLOCK BA8 METER VELOCITY
POINT TIME TIME READING HEAD
» * 'CLOCK)
1NIT 0 1045 565.194
E-02 *22lo 1107S ^584.000 1740
E-03 . 33.0 1248 595,720 1.045
"f 	 "E-04 " " -*1 44.0 1417' 608.600 	 1.150
ro E-05 55.0 1428 620.000 .950
W £-06 66.0 1530 632.000 1.060
' E-OB ''*'•"'' BS!O 1654 655.000 .920
M-01 99.0 1705 669.000 .695
	 ' 	 W-02 	 110.0 ' 1855 	 676.500 -.843~
N-03 121.0 1906 688.750 .930
M-04 132.0 1923 699.320 .922
N-06 154.0 2059 722.000 1.030
H-07 1*5.0 2109 735.000 1.100
W-08 " 176.6 2121 	 " 746.004 "" .950
TOTALS 17*.* 180.810

''"*""
ORIFICE PRESSURE
DIFFERENTIAL

STACK
TEMP
VHIE
RUN NUMBER
PROBE LENGTH > TTPE
NOZZLE 4-1221 I.D.
ASSUMED MOISTURE
• AnnC VOX NUMBER
METER BOX NUMBER
PETER HEAD OIFF.
PROBE HEATER SETTING
HEATER BOX SETTING
K FACTOR
E8L-1
5 FT CLASS
.258
3.0
113
F10
1.80
3.
3.
tlT2.
DRY GAS METER PUMP SAMPLE
TEMP VACUUM BOX TEMP


7
IMPINGER
TEMP
lin.ncoi (UCH.F) •• iDE«.rj • iin«*<«r ivev.rj iwcv.rj
DESIRED ACTUAL

2.95 2.95
4.12 4.12
4.60 4.60
3.80 3.80
4.18 4.18
4.32 4.32
2.74 2.74
1 3,32 3.32
3.64 3.64
3.63 3.63
4.09 4.09
4.33 4.33
3.70 3.70



93.
94.
90.
91.
94.
3k
90.
91.
90.
88.
88.
86.

INLET OUTLET

94. 89. 2.0
100. 90. 2.0
88. 89. 2.0
91. 89. 2.5
96. 91. 2.0
y '»' ^3^B ""
89. 87. 3.0
86. 82. 3.0
83. 81. 2.5
80. 80. 2.0
83. 80. 2.0
89. 80. 2.0
84. 76. 2.0
74. 72. 2.0
-


25o!
23tU
250.
250.
250.
250.
230, ~
250.
250.
• 9*i
250.
250.
230?



60.
61.
60.
46.
48.
55.
61.
61.
61.
61.
•*•• • f f
61.
60.
60.
. .^
_
'
V "• ''•'*?*'' •'
v
"
ts











V

-------
           PARTICIPATE FIELD DATA • RESULTS TABULATION



PLANT- NAME AND ADDRESS               TEST TEAM LEADER
'?' !'" ""."V 	 " ' !' 7'!" " ' " ' '
f PRESTOLITE MANCHESTER IOWA
TEST

	 TEST
TB
•'• ' ' • TF '
TT
NP
ON
CP
• , PH • '•
1
**
. „ „,..,, y p| ,, .
VMSTD
VLC
VNC
BNO
FMD
PC02
P02
PCO
PN2
MD
NNS
E8L-1 ENTOLETER SCRUB OUT
-.. .^p ,.. -
DATE 	
TIME-START
NET TIME OP TIBt, HlM^f^
NET SAMPLING POINTS
SAMPLING NOZZLE DIAMETER
PITOT TUBE COEFFICIENT
"•'."-'.? AVERAGE ORIFICE 'PRESSURE-,' •:*«.•!»
DROP
"" 	 " VOLUME "OF DRT" GAS SAMPLED "'" 	
AT METER CONDITIONS
VOLUME OF DRV 6AS SAMPLED
AT STANDARD CONDITIONS*
ft TOTAL H20 COLLECTED IN
VOLUME OF NATER VAPOR
AT SlAnDAttO CONDITIONS*
PERCENT MOISTURE BY VOLUME
MOLE FRACTION DRV GAS '
rlHtlNT Cue BT VUL.f DRY
PERCENT 02 BY VOL., DRV
"•;• •••• • • • • - HJE ".' •" "•>"•' • • •"'", '
PERCENT CO BY VOL., DRY
PERCENT~N2 BT" VOL"., DRY
MOLECULAR NT-DRY STACK GAS
MOLECULAR NT-STACK GAS
PROHASKA ' ''*""'' ."'"' '.'"'•'' ' ]

ENGLISH UNITS METRIC UNITS
	 06/08/8! "" 06/08/81 	
1045 104S
•til - eiei + ,.--,..
176.6 •' 176.6
16 16
.258 IN 6.6 MM
.80 .80
_ ,..»,... ^
180.810 CU»FT 5.120 CU»H
1 ' 85tf9 P ii1.'1."1 " '! Jff.O ' C ' " "" 	 »•-•". ..u1 w'1.""11" »• 'I»










-------
 PB



 PSI
P«|l MM III


 PS



TT
 BAROMETRIC PRESSURE


 8TAT1C PRE8 bF STACK BAS
f^+ •'-'••— -v1 /-^S' ^S^^-i^p-"-^^^

 STACK PRtS, A||«
                                                  28. S3  IN-H6


                                                   -.50  IN-M20
                                                      724.66   PM-HG


                                                      •12.70   MM-H20
       VS
 AVEWA6E STACK ItnP


 AV6 STACK BAS VELOCITT
                                                         fN«MO
                                        FP8
tis.rs  MM-MB




 16.5   UPS
       asifO     Sfatfc FLo" R*YE» OitV<


       08        ACTUAL STACK PLOW RATE
                                481.   80-1N             .510  80-M


                             57760U    ^CFH    ~  16556.     SCWT


                             650278.    ACPH       18414.     ACMH
       MN

            V * V i
 FILTERABLE PART.

    I*T
                                 10.*
                                                                 10.2
                                         '
       CS
FILTERABLE PART*
       PMR       FILTERABLE PART,

                   EMISSION RATE
                                      '" '   *
                                              •OSO« 6R/OSCP*
                                   .074   LB/HR
                                                        2.050 N6/08CM


                                                          .03  K8/HR
40


41



• t
                                                                          "W

-------
                                                                                                                                               .:• /
             EXAMPLE PARTICIPATE  CALCULATIONS  TEST NO.  ESL-1

                  ENTOLETER  SCRUB   OUT
      VOLUME  OF DRY CAS  SAMPLED  AT STANDARD  CONDITIONS	—

      VMSTO « (17.647  *  VM * V * (PB «• PM  /  13.6)] /  (TM * 460.)
                 17.647  *   180.810 • 1.044  *  ( 28.53 *  3.727 /  13.6)
      VMBTD  «  [[[	175.754 DSCP	      	
                 '              '   (86. * 460.1         ~"        	   "	             "~"  "	            "     	"  "" '


I'"!'."' i... .IP   i.   . . 	    	  ,'  i.iii u,v  11. 	;  . _ "      i.	'"•	    *'  . '   v	I '  '         	       —"	•	 * 	 »' " 	r	       ' •	'	 '1 	

      VOLUME OP MATER VAPOR AT  STANDARD CONDITIONS

      VWC •  ,««/o7 •VLC                        '   '          ~~~~~          ~~~'   ~~     '     ' ""           '       " ' '  	"	  "

      VWC •  .04707 •  191 • •    5.02 8CP		__„.	_______________
•w : ~ ~~:"  - '   ";: l~~.   -  •• r  " '": :~:" r^i- V ?'"fl>^ - -^^^^;   ' \r: • ,* ^' "' i?^ -'"~~ ' :'"'" '" '"   * '"*^""' *" "Jl "" ^ "" ^~"  "^   ' "  "  ^ """   '• "v   :  ^s-w"*^,^4 j-.-'i'-k1              —«  ^    - -^ ^     .. ;I


	PERCENT  RQisruRE  IN STUCK GAS';~                            ~~

      BMP »  (100. * VNC) / (VM8TD •» VMC)	__________^	      		
___,,,,,   . ..  	...;    ^    .   ,      ,  ^^    ,_,     .   :  ^,   ,     ^          ,_    ,        ^   ,   ,      &w	v- :  ••-••X-'"     :            '       • • -'^-ty
                 100. *    S.OI
	BMP »  --.«...»-..-...«.».».«.««..«i »  g.7» PERCENT	  _    __	    _	
~*pi                175.754 »   b.w2        '                          "        '" ""	"	~ '          "                     	          '


 rr\                                             	                                                      ii_»-.._ 	  ..mmx -m ~               	

      MOLE FRACTION OP  DRT STACK  GAS

	Pf»O~»~(100. • BHO) / 100.	—-_	  	                     	


                 100. •    2.8
„	v pup m  mmmmmmummmmmmmmmmmmmmmm .m >jjili—r	"•:••". .. • '••,•» .-, ..'•	••	-^	'	'  "W*^i  ;•••••"-""""	'	'	-if
                      100.




	AVERAGE  MOLECULAR WEIGHT  OP DRY STACK GAS  	    	
.'.'.-''W  "	™!	'	~	~—".—' !J»».«-c»'	"	r-r—•	r.	"~~^?	^—-7-	•:!•$.-•	.-' -*. - •-?-  •••  	-	.;•	—'	 •" '^'T?'"-' .y.-r'"g» "'V ""' ' 'ST^"'	r~^	.  ' • •';)'•• I!|;?..»','J»1
      MO •  (PC02 • .44)  * (POt  *  .32) » (PN2  » PCO) *  .28                                   '

      MD •  (  ;00*44/100) '» (20.9*32/100) V  ((79.1» ^OJ"T"~28/199~v    28.84"^         •     •   •         —_—,—.		-  -            	—-




      MOLECULAR WEIGHT  OF STACK GAS                                                                                                               '

      MWS *~MD~* (Ti •  (0WO/1A4))  * T8". *  (BHU/100)    "  ~~                                          ~                 "

      MW8 «  28.84* (1.  •{ 2.78/100)) » 18. *  (  2.78/100)  •   28.54




-------
 STACK CAS VELOCITY AT STACK CONDITIONS
 DELP « SUM. Of THE SOP.TCVH •  (T3 *  460.))
*•  •.'..£• .     • -s  ,-   -•••••:,• -v • s«vw*«»r7  *T ••'  •    5^    •.-•
 VI * §8.4* * C*» * OIL* / tlOHf(MNS  * M) * f»NT8)

 V8 • 85.49 * — .00 "» — 560.698 J
                                                           TB
 STACK 6AS VOtUMftRfcCFlON At STACK CONDITIONS
US • V8 * AS * 3600/1M	'	

 08 *   94.07 *   401. 3600/144 •     690270.  ACPN
       K«3
                           JT lVAH6Aht»
 OS8TD * 17. M7 * OS » PS •  Cl. •  (INO/IOO))  /  (TS  *  460.)
      •     tf»MT «     »S0tt», *  *ft.49 *  11.  -  (  2.78/iOt))
 «8tTO • *«i— —•—••••——»••*•••»-•—•*———————
- — - (  90. * 4bO.J
                                                                    S77601. 8CFH
»
i.
         I80K1NCTIC
 tso
(309. 50* (
                           ))•((».
                                            107. )*(   100.010*1 .044*( Z0.S34(    3.727/13.*) )/(  0ft.+4tO.)))
                                4    177.  «
                                1     .    :•>
                                                54.07 *   20.4* *  .190 «   .«90
 PAKTICULATE LOADIN6 — EPA METHOD 9  (AT  STANDARD CONDITIONS)
 69 • 0.001 * MM * 19.41 / VMST6

            I'2.9 * 19.43 /
                                                 .600
 PARTICULATE LB8/HR *« EPA METHOD I

     * CS »dSSTD/119.43 • 493.6)
          PMR •
   .000 *
                      977601. /  (19.43  *  493.6)  •
                                                        .02
                                                                                                                                       r.
                                                                                                                                       71

-------
FIELD  DATA
f r 	 -r- 	 PLAN? •• 	 "•'•"•• ' ' - •
: SAMPLING LOCATION

SAMPLk TTKt
OPERATOR
AMBIENT TEMP
.(DE6.F)
STATIC PRESS. (IN. H20)
FILTER NUMBER(S)
1
1
4
IS
STACK TNS IDE DIM. (IN)
PITOT TUBE COEFF.
THERM. NO.
	 •"' PRtSTOLITI
ENTOLETER
LEAD M12
PROHASKA
66.
C6.0*
-.50
0002281
24.75
.80
128
SCRUBBER STACK




UMI ••"'• 	
:.A \





DATE 	
RUN NUMBER
PROBE LENK
NOZZLE
ASSUMED MO
METER BOX
METER HEAD
TtrT~TTP
t I.D.
ISTURE
NUMBER
DIFF.
ESL-2
E 5 FT 6
.254
3.0
115
F10
1.80
?


PROBE HEATER SETTING 3.
HEATER BOX SETTING 3.
LEAKAB£ • .wiu trn •• iv.v
METER CALIB. FACTOR 1.044
READ ft RECORD DATA EVERT 8.0 MINUTES
i* TRAVERSE SAMPLE
,. POINT TIME
70 '
21
" INIT
, j r •i?;-"- it-gi
>. N-02
> N-03
I'. CO N-05
,0 N-06
I', N-OB
E-01
„ E-02
E-03
,. E-04
I. E-06
E-07
k-08
E-08
E-07
1! TOTALS
AVERAGE
*ft
47
48

0
16.0
24.0
aolo
48.0
64.0
72.0
80.0 "
88.0
96.0
112^0
120.0
136^0
144.0
144.0

CLOCK CAS METER VELOCITY
TIME READING HEAD
CLOCK)
815
831
839
855
903
925
943
953
1009
i^iJ ;--.-*
1025
1033
1041
1049
1057


ivu.ri.j im.neuj
747.040
76U300
769.900 1
776. 75«
787.710
796.800
" 805. Ovo
814.843
822.150
' 630;000
839.220
848.000
667.000
872.000
684.640
893.700
902.285
155.245


!830
t.100
.100 	
.100
.100
.1 vO
.050
.730
.850
.100
.150
. i vv
.000
.050
.970 "
.100
.010


in.nv

ORIFICE PRESSURE
DIFFERENTIAL
iiw.n
DESIRED

3.20
4.20
4.30
4.30
4.40
4.20
2.90
3.40
4.50
4.70
1 4.50
4.10
4.30
4.00"
4.50
4.08
4.03

*UJ '
ACTUAL

C.3V
3.20
4.20
4.30
4.30
4.40
4.20
2.90
3.40
4.50
4.70
4.10
4.30
4.00
4.50
4.08
4.03


STACK
TEMP
Oltmtf

66. "
98^
95.
92!
91.
100.
93.
89.
93.
92.
91.
91.
95.
98.
93.

K FACTOR
DRV GAS METER
TEMP
(ufiw.P)
INLET OUTLET

•t. •*«
67. 63.
65. 64.
82 . 66 .
87. 69.
92. 72.
94. lii»f;
95. 78.
94. 64.
^»r; 8*.
96. 66.
100. 88.
96. 66.
99. 89.
100. 90.
TOO. " 90.
99. 90.
97. 88.
90. 80.


PUMP
VACUUM
2223.8

SAMPLE IMPIN6ER
BOX TEMP TEMP
limn*) 'ivBV.rj vucK.rj

6.0
9.0
9.0
10.0
10.0
"*'"' '9.»
9.0
6.-0
7.W
9.0
10.0
'9iO
B.O
9.0
*.o
9.0
9.0
8.4


2SO.
220.
24TT~
260.
270.
250.
250.
275.
250.
250.
K70.
300.
"300;
275.
250.
261.


so! "
56.
62.
66. >•
60.
60.
50.
55. .,
50.
50.
60.
S:
52.
S5.

50
91
B2
J
4
i 	







i












»
;-]}

-------
           PARTICIPATE FIELD DATA I RESULTS TABULATION



PLANT- NAME AND ADDRESS               TEST TEAM LEADER
f IT*' .;'
PRESTOLITE
MANCHESTER* IOWA PROHASKA
"-'*"' '«•'*• ' :- : .- • i f>
TEST ESL-2 ENTOLETER SCRUBBER STACK ;
K 1?. '- •- : • •*>.
T£St DAtt
TB
. •'*?* TF " W~"*
i
TT
! NP
1
•-.;"' y " •»?-+.|P.tt -'-M-1?1
0
ON
! CP
4
i * - FP • •* ^J>*^
• . „
* > -i" '
- ro
. IQ
~7 r • • • 1 h " \ ? J - -"' V!?1!
! VMSTD
4
! VLC
! VNC
O
1 8NO
1 :,"^ / *?/"-.> -^a
FMO
^ (
	 	 PCOZ " ' ' "
• 7
.. P02
4, ^'o'fj* ^'•(.-•^ •
PCO
fll -^ _ , ,
.1 • PN*
•>
M MD
KB ?• P -,••"?
•• MN8
5'
s. •••". ;.v j-.jys" [»'•? .y*?.-"-?' u '.wf- i.ia«"ii:r •- »r • :•• ;••*'» •
,-rt '>,->.• " ' ' EN8HSM UNITS
TIME-START 813
NET TIME OF TEST, MtNi*p |T 144.0
NET SAMPLING POINTS 18
8AMPLIN6 NOZZLE DIAMETER .234 IN
PITOT TUBE COEFFICIENT .80
DROP
vuiund OF 6tV CMS SAMPLED* 1^3.243 £U-FT
AT METER CONDITIONS
UV^^wJ^^K^P«W^T^w^^H*^^.w^^^^^^^^«^^^^^^^^^^^'^^^^f '' •••' • '^
' ^.,
VOLUME OF DRY 8*8 SAMPLED 131 .83* SCF
AT StANbARD tOwOillOH*"
TOTAL H28 COLLECTED IN 99.7
VOLUME OF NATER VAPOR 4.893 SCF
AT STAfcOAftb C0ni)i ( iuni*
PERCENT MOISTURE BY VOLUME 3.00
MOLE FRACTION DRY «»* J' I .970
PERCENT C02 BY VOL.r '0*T' "" 	 .00
PERCENT 02 BY VOL.» DRV 20.90
PERCENT CO BY VttOrDHt -'^ ' -}• '.!,»•"
MOLECULAR NT-DRY STACK OAS 28.84
MOLECULAR NT-STACK BA8 28*31
METRIC UNITS
Ofc/Ol/Bl n
813 ','.
1037 " 	 	 " '" ' "' ""•' "' " '•'";"~ • '" T . -1"1 ':i»
>«4.0 . ^
is ;;
*.3 MM |
.80
j

4.196 CU«» ~*
4.300 8CM
99.7
.133 SCM ;;
3.00 ;;
-•• ' .970 '" '' "" '" " '' ". ' ' ' "•«
.00
20.90 )I
'5'"^' •••' ' . * * """^T??' ' • "^
7">.lO »
X
28.84 ;;
28.31 ;;

-------
PB BAROMETRIC PRESSURE
PSI STATIC PRES OF STACK CAS
F;:!"'::. •-,-.-. ,;,-. ....... , ,, .„- 	 -y -i -
, P3 STACK PRES, ABS.
4 TS AVEHA6E STACK TEMP
! VS AV6 STACK GAS VELOCITY
i AS STACK AREA
10 uaiTu &fACK FLOn RATE, DRV*
!! QS ACTUAL STACK FLON RATE
!! ISO PERCENT ISOKINETIC _. .
it MN TUTAC LtAD
.7 M6. EPA 9
„ • "!:""CW"'-> •'•*-' -•* TtTIt LEW-":1™*1 '?• >-1 %4W""W- ',
" PMR TOTAL LEAD
EMISSION HATE
MN FILTERABLE PART.
C8 FILTERABLE PART.
u PMR FILTERABLE PART.
Q EMISSION RATE
' * 68 DE6 Ft 29. »2 IN«H6.

:'"'' '^fft *•' *: ",. 	 vf* . ' •"•*?«'•
.
-*'• ';•-.•'•'_• ' -" .''^ns.%* t"J" ^^ "ni:/;r ^'' / '*v-.^*J '
1

: .-,.,,, .^ .-, • ..-:;,^;W-*,--.«ri- -r

.
28.64 IN-HG 727.46 MM-H6
-.50 IN-H20 -12.70 MM-H20
28.60 IN-H6 ' ' 726.92 MM-H6
111 93. F 	 34. 	 C 	 "" 	 " 	 """" " "' "' 	 "'
56.3 FPS 17.2 fPS
481. 80-IN .310 SO-M
599420. ' 3CFH 16974. 3CMH
677000. ACFH 19171. ACMH
100.2 v 100.2
5.4 5.« i
• • • '• ;VOOft 6R/DSCF* 	 	 l.IVS fB/DBCH "•' ,-.--,-. '«•;!« •«i.v.mv " ' • - • • 	
.047 LB/HR .02 KB/MR ]'t
51.5 51.5
.0092 6R/D8CF* 11.978 K6/D8CM \\
.448 LB/HR .20 K8/HR
., . . ....... . . . . • ,.,..„ ^ ......... •

"' l'"-'- •"""' ' " 	 ' ,^^-^r • • ^
>«
, «. . ... . . -. • ,. • ,..--.- - .^. . • .-^. ^

,^ ' ••-' " - ' ' -^;^^.-c.- •-. — -JTjj
70
74

-------
      EXAMPLE PARTICULATE  CALCULATIONS TEST NO. ESL-2


           ENTOLETER  SCRUBBER  STACK
         "VOTOWF"
-wr
                           At  St»r*d»Rn CONDITIONS

VMSTD • (1T.M7 • VM  *  T  * (FB » f* / 13.6))  / (TM * 460.)
»

»4

          17.M7 *    14S.M5 *  1.044 * (  88.64 * 4.027 / 13.6)
VM8TO •* •^**«.«»MM»..-.....—.....................—..—— .
                                                                              131.856 DSCP
VOLUW Of ItAtER
VHC » «47»  *             .  i,..,


VMC « .04T07 *   It*.  •    4,*» Stf
                                                       ^^^^^ "* -^-- '•'*•- -^-
                                                                                                    ""^PWW^V
        MoJtltuRE  in  StAcn  rtAi
BNO • (100. t VWC)  /  (VMSTO * VNC)
AVERA6E MOLECULAR NE16HT  OF DRY STACK CAS
                                                     Mwwaw
                                                                                                        •jiiHH"1:.. <-'i'P.'J
                                                                                                                   TTW|
MO
                                               .0) « 28/100 H	2«1
HM8 • MB *  Cl. -  1BWO/10UI)"» IB. * (BUD/lDm
MNS
                        (I, -( S. 00/100))  *  IS.  •  (  3.00/100) •   28.51

-------
 STACK 6AS VELOCITY AT STACK CONDITIONS

 OELP • SUM. OF THE SQRT(VH * (TS * 460.))
 VS « 85.49 • CP • DELP / (90RT(MM3 * PS) * PNTS)

~VS » 85.49 »	STBim—423.049 / {5ffRTTTtV5T"» 2fr;60)  r  T8."""«5B729 TPS
 STACK GAS VOLUMETRIC FLON AT STACK CONDITIONS

 08 K V8~* AS «~ 36(Hm44	
 OS *   56.29 *   481. 3600/144 •     677000. ACFH
 STACK  6A3 vOuuwtc FLuH *

 OSSTD  * 17.647 » 08 • PS » (1. • (BMO/100)) / (TS » 460.)
           17.647 *     677000. •  28.60 *(!.-( 3.00/100))
 OSSTO • ——••••<•<'-••«-»«—'>—••-•«••——————•—«•«••»-»•• «  ___ 599420.  8CFH
                           * «60.)                                   ........ "
 PERCENT ISOKINETIC

 iau • (305.56* (l4»4ftO.))»( {0.002669«VLt)»lVH*Y* IkB* (pn/13. 6j )
        (30S.S8*(  93. »460.))»((0. 002669*  100. )*(  155.245*1 .044* (  28.64+(    4.027/13.6) )/(  85.t460.)))
 lav
                                    144. *     56.29 *   28.60  *   .254  *   .254
 PARTICULATE LOADING — EPA METHOD 5 (AT STANDARD CONDITIONS)
 C8 » 0.001 • MN * 15*43 / VMSTD

~C5 • u.uuisS.4*15.43 /
 P ARTICULATE L8S/HR •>• EPA METHOD 5

                    (15.43 » 453.6)
 PMR •     .001 *     599420. / (15.43 * 453.6) •      .05

-------
                                                      FIELD  DATA
~5AKPLt~
 OPERATOR
 AMBIENT  TEMP.(DEO.F)
                               PROHASKA
                                64.
RUN NUMBER

PUUBF tEHGTlT
NOZZLE 4-1161
                                                                                           tTFT
                                                           I.D.
                                             ASSUMED MOISTURE
                                                                            ESL-3

                                                                          ~~5~T00T~ttrS»
                                                                            .258
                                                                            3.0
      STATIC -PRESS. UN. Ht»0)
      FILTt* NUMBER (8)
 *.SO
1)002233
                                                                       SAMPLE BOX NUPVCIV
                                                                       METER 80> NUMBER
                                                                       METER HEAD OIFF.
                         F10
                         1.80
      PITOT TUBE COEPF*
      THERM* MO.
  .SO
138
                                                                       PROBE HEATER SETTING      SO.
                                                                       HEATER BOX SETTING       250.
      METER CALlB. FACTOR^,   o, 1,044
      READ • RECORD OAT A E%tR>.:J.O MINUTES
                                             K FACTOR
                                                                                               ttftr.s
TRAVERSE  SAMPLE  CLOCK
 POINT     TIME    TIME
•AS METER  VELOCITY  ORIFICE PRESSURE  STACK
 READING     HEAD      DIFFERENTIAL     TEMP
                                          ORT GAS METER  PUMP
                                              TEMP      VACUUM
                                                                                         * SAMPLE
                                                                                          BOX TEMP
                              IMPINGER
                                TEMP

-------
           PARTICULATE FIELD DATA « RESULTS TABULATION



PLANT- NAME AND ADDRESS               TEST TEAM LEADER
* - .-:.
PRESTOLITEf MANCHESTER PROHASKA
TEST

ESL-3 ENTOLETER SCRUBBER STACK
ENGLISH UNITS
TEST DATE 06/10/81
TB
' TF
TT
NP
-• ' - T 	
ON
CP

'f VM
1
U)
VM8TD
VLC
VNC
BNO
FMO
P02
PCO
' " PNZ
MD
MMS
TIME-START 741
TIME-FINISH • ' "•* i*J^ " •
NET TIME OF TEST, MIN. 163.1
NET SAMPLING POINTS 25
'•"' HETER1 CALIiRlUOlTFAC'YOir*"" '""" ' "1W* 	 •"""'"* 	 """"
SAMPLING NOZZLE DIAMETER .258 IN
PITOT TUBE COEFFICIENT .80
DROP
VOLUME OF DRT GAS SAMPLED 170.084 CU-FT
AT METER CONDITIONS
'"••*" AVERUM VMS METER TCMP , , \r ••• • 'itu F^ ' ". 	
VOLUME OF DRY GAS SAMPLED 168.86S 8CF
AT STANDARD CONDITIONS* ' ' 	
TOTAL H20 COLLECTED IN 113.3
'' 	 " 	 IMPINGERS AND iltICA -»ltV"l'i";"r'' ""•" "' "".'"' ''' 'F^~ .""•'
VOLUME OF MATER VAPOR 5.333 8CF
AT STANDARD CONDITIONS* " "
PERCENT MOISTURE BY VOLUME 3.06
MOLE FRACTION DRY GAS .969
PlrtCitoT C02 BY VOL.r DRt .00
PERCENT 02 BY VOL., DRY 20.90
PERCENT CO BY VOL., DRY .00
PERCENT NZ BTVOL.. DRY 79iIO
MOLECULAR NT-DRY STACK GAS 28.84
MOLECULAR NT-STACK GAS 28*50
1 K--, -

METRIC UNITS
06'10/81 ~ .... -.
741
163.1
25
6.6 MM
.80
-f




4.816 CU*M ' " " 	 ~ 	 ' ' " '
>•'
4.782 8CM
113.3
.151 SCM
3.06
.969 ' ' ^ ' r 7T^
~ 	 .00 • •• 	
20.90
.00
79.10
28.84
28.50
•*i







-------
PB BAROMETRIC PRESSURE
P8I STATIC PRES OP STACK GAS
. " PS / STACK PRES, ASS*
i • . • 4.
. T3 AVERAGE STACK TEMP
« VS AVG STACK GAS VELOCITY
\ AS STACK. AREA
* - ..• •*<$* •'-•• * *
• . , .. . 	 ... .„_:-, , , ,,.- ,
10 OSSTD STACK FLOW RATE* ORT*
!t 08 ACTUAL STACK PLOW RATE
"' '"'; "ISO " ? PERCENT ItO^Wt^Ci^^jl
-. . , . ,.^im
i. MN TdfAt LEAO i . . ^ ^
.» . M6. EPA 5 ,. .-i -: "f,
i. • ':'''.
,,r • C»-'- .^^^'^IA^lI»»^lPPP*l4iB|*|p
zo • •••;•; «'•• ; ¥;i "4i ' •**
PMR - TOTAL LEAO ' ^
>: EMISSION RAfE
» MN * FILTERABLE PART*
"'^ C§ ' "...o ^ItTeHAttB/PART^';.^-';;^!
» u> PMR FILTERABLE PART*
,. <" EMISSION RATE
« -'•'.' '•"": / \-\ 4''! ^ ?<' ' '
»«
Ji , ' *r * V' '
•o
•f
•t
-V • ;^!v":"- s'v^ !^:w': ?
4f
4T _ ' ' . ' ;;..'.
il .-<*•••/•
4t^^^*..-,;i^.fr.--,-:,^V^li^Mp^^lj|Mjjptl!^^^,^'
•'•' ' ;;:; .. . ,,^!;; . 'j«;w'^r^. .:
• 2
Mj ....
"
28.79 IN-HG ' 730.29 MM-H6
>
•.90 IN-H20 -12.70 MM-H20 l
28.71 IN-HG 721.32 HM-HG J
	 "" ""So.J - F •----• ' Jz. c " -.---. §
94.3 FPS 16.9 PP8 I
481. 80-1N .310 SO-K ;°
582625. SCFH 16498. 8CHH ~ '" ~^
692897. ACFM 18487. ACMH \\
*;•'/ *••! ' *•«» ' .v- -Vj, . , '
If.: . . & -f :::
4.3 4.3 ..
>.}•>.:•' ? • '.'••. ' ,,
.033 L8/MR .01 KG/MR 	 ^
>•
10.3 10.3 ;;
:»,"fr-' -. •• • • '• -p,4
,i,^ .0001 OR/D8CF* t.134 KG/OSCN ]\
.078 LB/HR .04 K6/HR >•
HjffTrHtW^'1- WfP^w"*- '•'•"-'."*&'*' •*• '•^''V.'flllM '','•'" '•""•I:-1 ••" '"•ln'^l"*P'!f»4i?. V 'Pi^MJl'.V •''.li'p!"^!1, ",!.•,. .pl{!!« ' *(. '- •- ' 1J'!*afr"'ff'«i

T t •• • • •••*• • « :'•. -••;•• • •.,-;•• . • •-., • •• ,„

• "v **'•"•". Jlv ^ ,'•'"•"• *
0
,^,_I;^^^, ,^,,,^,,r.^, ,,, . ,>, ,..^^w^:¥,,- ... -1WJ
1
,,,,,,^ ,, ,,^.,t . . . , . ,, . . , -j-

-------
                EXAMPLE PARTICIPATE CALCULATIONS TEST NO. ESL-3


                     ENTOLETER SCRUBBER STACK
         "VOLUME OF PRT'tAS SAMPLED AT 8TANP«RO X0N01T101»3~	


          VMSTO * (17.647 • VM * Y « (PB * PM / 13,6)) / (TM * 460.)
                    17.647 *   170.064 * 1.044 * ( 36.75 t 3.784 / 13.6)
          VMSTD • -...•.—••—«—.-•—.«•••-•-««.-—————•---• »    166.863 DSCF
          VOLUME OF MATER VAPOR AT STANDARD CONDITIONS
          VNC • .U47V7 * VUC


          VNC • .04707 *  113* •   5.33 SCF
          PtHCtNT HDISrUHC IN BINbK


          BNO » (100. * VNC) / (VMSTD * VNC)
   OJ
   (Ti
                    109. *   5,33
                    ..—-.————— .»  3.06 PERCENT
                     166.B65 T	5VJ3	
          MOLE FRACTION OF DRY STACK CAS


          FNO •(100. • 6wO)/ 100.
                    100. •3.1
                        RWWJM

                         to*.
          AVERAGE MOLECULAR NEIGHT OF DRY STACK GAS
          MO * (PCOZ * ,44) * (POZ » .32) * (PN2 • PCO) * .28
                  .*
I
          MOLECULAR NEIGHT OF STACK GAS

         ~MW*~Minr-(i. - (BHO/nnm + iTrT

          MNS •  28.84* (1. -( 3.06/100)) * 18. • ( 3.06/100) •   28.50

-------
        STACK 6AS  VELOCITY  AT STACK CONDITIONS


        OELP • SUM.  OF  THE  SORTCVH * (T8 * 460.))
        VS • 85.49  » Cf»  *  DELP / (SORT(MN8 * PS)  * PNTS)

                                        rsourr*B.5o~» 2s
                                                                        FFS
        STACK 6A8 VOLUMETRIC  FLON AT STACK CONDITIONS


        OS * VS * AS  *  3600/144	"	—
        OS •   54.26  *    461*  3600/144 •     652857. ACFH
        STACK CAB VOLUMETRIC FLO*"AT*llHlP>ffD CONDITIONS	—


        OS8TD • 17.647  •  08 • PS * (1. » (BNO/100)) / (T8 * 460.)
   >

   u>
PEMCENT ISOKINET1C


180
                (305.58*C   90«*4*0.))*((0.002669*  113.)*(  170.084*1.044* ( 28.75«(    3.784/13.6))/(  79.»460.)))
                 *  '" '* jL '  vi>   ' .-j-
                !'*<•••••*   *  ".••£>•'•• us.
                                                       94.28 *   28.71 *   .258  *   *>58
        PARTICULATE LOADING  •- EPA METHOD 5 (AT STANDARD CONDITIONS)
                  i,      '-"? -  •1W'.>»' 5-rWPF^.;.- ^f TjiT i' , .,   T'"jSir.

        C8 • 0.001 • MN  • 15*437 VMSTO             ^
        C3 • V.VV1 *
                                          IBB.0ft? •
                                                        .600
r-^
                         .       .,,

        PARTICULATE  LBS/Hft ** EPA METHOD 5
        PMH « IS  *"OS8TO  /  115:43
        PMR •
.000 *     562625. / (15.43 * 453.6)  •
                                                       .03

-------
FIELD  DATA
S • - . . : •



PLANT""1 ' '' 	 ' "" ."
SAMPLING LOCATION
SAMPLE TTPE
OPERATOR
AMBIENT TEMP.(OEG.F)
STATIC PRESS. (IN. H20)
FILTER NUMBER(S)
STACK INSIDE DIM. (IN)
PITOT TUBE COEFF.
THERM. NO.
	 	 PRE8TUI.IT
ENTOLETER
PART MS
PROHASKA
67.
••*•- •• :26.64
-.50
0002286
24.75 '
.82
129
r W«TfCHEBTMi '
SCRUBBER STACK


.00


IOH A





UAIE
RUN NUMBER
PROBE LENS
NOZZLE
ASSUMED MO
METER BOX
METER HEAD
Ttrr-TYPE
1 I.D.
ISTURE
NUMBER
NUMBER
OIFF.
ESP-
5 FT
.258
3.0
F82
1.76
1
GLASS

PROBE HEATER SETTING 290.
HEATER BOX SETTING 290. \
!! METER CALIB. FACTOR 1.003
READ ft RECORD DATA EVERY 8.0 MINUTES
',' TRAVERSE SAMPLE CLOCK CAS METER VELOCITY
,. POINT TIME TIME READING HEAD
,, ' •"•! •'..;:•'• no*
INIT
E-07
E-06
„ j> E-05
„ 1 E-04
oo E-03
» E-01
„ N-06
„ N-07
N-06
N-05
I! N-03
„ N-02
40 N-01
., N-01
N-02
TOTALS
AVERAGE
47
CLOCK)
0 619
16.0 839
24.0 643
32. v 4>5i
40.0 699
48.0 906
"•.. . ~' 3O.W ' Tl 9 • ' *
64.0 921
72.0 929
BO. 4 ^1£
66.0 992
96.0 1000
I W»W ' ' two '*"? '•"
112.0 1016
120.0 1024
128.0 1040
136.0 1048
144.0 1096



730.682
750.700
760.000
7&4.250
779.030
786.550
604.962
614.570
824.650
634.620
644.440
<>05J*93v
663.700
672.000
880.390
666.000
699.107
166.429 ' :'



1 4"A6o
1.200
1.090
1.000
1.100
1.090
.700
1.100
HT9T
1.100
1.050
i.wuo
1.050
.600
T7W
.900
1.110


ORIFICE PRESSURE
DIFFERENTIAL
 .



















-------
           PARTICULATE FIELD DATA ft RESULTS TABULATION



PLANT- NAME AND ADDRESS               TEST TEAM LEADER
/s g^r • • •- •
t ' PRESTOLtTE
MANCHESTER/ tWA '••
PROHASKA
• ,' 'I; '':•',' ^ '
J'_ ' *< ' T " - • T'..f ,|
.' TEST E8P-1 ENTOLETER SCRUBBER STACK
7 i ' • - 1 ""'•$•
.. ttS'f DATE
.1 TB
ii ' PPV" Tr" '!*" vV-
!! TT
.' NP
„ ON
CP
«
;v"T-' w " ' v»--p^:'
^ • 4 -i-
1
u>
VMSTO .
VLC
VMC
BMO
*• <-,,, ... -.,
P02
PCO
( '' • EN8L18H UNITS METRIC UNITS
TIME-START
MirTIME§W mtT*3^
NET 8AMPLIN6 POINTS
•AMPL1N8 NOZZLE DIAMETER
riTOT TUBE COEFFICIENT
OROP ' ' ' Ht
JJIL±^ _• _aj_j_i JM. j- ii H UM.J mA
VOLUME UP DHT B«5 SAHfLCD
AT METER CONDITIONS
VOLUME Or DRY 8 AS SAMPLED _,
TOTAL H20 COLLECTED IN
VOLUME OP HATER VAPOR
PERCENT MOISTURE BT VOLUME
MOLE FRACTION DRY 6A8
PERCENT C02 BY VOL.* ORV
PERCENT 02 BY VOL.» DRY
PERCENT CO BY VOL. • DRY ''"
pNg "PERCENT N2 BT VUL.r DRY
MO MOLECULAR NT-DRY STACK 6A8
MM3
IT
MOLECULAR NT-STACK 8AS
06/09/
819
%WI09» "' ' '
18
.858
.82

160.49*
124.7
9.870
3.53
<96S
;oo
20.90
.00
28.84
28.49
81 0
819
144
18

.0
'
IN 6.6 MM

1MNIO ' 10 V
CU-Ft 4
SCF 4
124
•K -X Jt
scr
3

20

28
"
.82
" *""^"
.769 CU-H ....
.545 8CM
.7
.166 8CW
.53
.965
;90
.00
.84
.45
K

o
14
11
1«
T •
t t
10
7 t
X
*
4
B
7
0
1
t;
4
•
7
4O
X
9
4
*
4f
4T
1O
94
• 0
• X
41
• 4
«t
K7
*•
:,

-------
PB BAROMETRIC PRESSURE
PSI STATIC PRES OF STACK GAS
»"" 	 '""" ' ' - - ,- - -: . ?
PS STACK PRES, ABS.
' 	 TS 	 AVERAGE STACK TEMP
VS AVG STACK GAS VELOCITY
AS STACK AREA
OSSTD STACK FLOW RATE, DRY*
08 ACTUAL STACK FLON RATE
ISO PERCENT ISOKINETIC
MN FILTENABLE PAttl
MG. EPA 5
PMR FILTERABLE PANT
EMISSION RATE
MN COND. INORGANIC
""* ' • - • TTT» '•  EMISSION RATE
MN COND. ORGANIC
MG. EPA S
C8 COND. ORGANIC
EMISSION RATE
MG. EPA S
PMR TOTAL PARTICULATE
EMISSION RATE 	
* 68 OEG F, 29.92 IN.HG.
,,.,,,., -^.v •:-;•; ••-•-•-

"• • -
28.64 IN-HG 727.46 MM-HG
-.50 IN-H20 -12.70 MM-H20
28.60 IR-H8 " 726.52 MM-HG
57.8 FPS 17.6 MP8
481. 80-IN .310 80-M
":Ktt259. SCFH 17309. Sg«M
694794. ACFH 19674. ACMH
...-;.-.. ... - - .--. -- - 	 ...-.....- 	 ...... _. .. ... ... . ^_
100.7 100.7
31. « Jl.4 -r- . . .
.264 LB/HR .12 KG/MR
.4 .4
.0080 6R/08CF* .088 MG/D8CM
.003 LB/HR .00 K6/HR
2.8 2.8 *
.0003 6R/D8CF* .616 M6/D3CM
;
•" 34.6 34.6
.291 LB/HR .13 K6/HR

^ ' ^ ^ ' . ' "' "" """'"" "^

•





;;















-------
       EXAMPLE PARTICIPATE CALCULATIONS TEST NO. ESP-1

            ENTOLETER SCRUBBER STACK
 VOUOHE" Or~DTTT CW~S«HFCEO" *T~STANDARD "CDNDITIOW

 VN3TO • (17.647 * VM * Y • (PB * PM / 13.6)) / (TM * 460.)
 VM8TD * —
           17.647 *   168.429 * 1.003 * ( 28.64 * 4.228 / 13.6)
                                                                    160.494 OSCF
 VOLUME OF HATER VAPOR At STANDARD CONDITIONS
"VWnr— 04707 * WLC	'	'——

 VNC  • .04707 *  125. •   9.87 SCF
 PERCENT  MOISTURE IN STACK BAB


 BMO • (100. • VNC) / (VM8TO • VNC) .

           100. *   9«8t
           —•••••«•-••-•***••**•• *  J.SS PERCENT
            16U.4V4 ?	5^7	
 MOLE FRACTION OF IRT «t»e
-------
 STACK GAS VELOCITY AT STACK CONDITIONS
 DELP * SUM.  OF THE SORT(VH « (TS * 460.))
 V8 * 85.49 • CP * OELP / (tQRT(MNS * PS) * PNT8)
 V8""«' 89.49 t  ,82 •—423.192 / (SURTt 28.49 • 28.80)—•  18. *	5t^T7 FPS
 STACK GAS VOLUMETRIC FLOW AT STACK CONDITIONS
 OS • VS * AS * 36UO/144	:	
 OS •   97.77 •   481. 3600/144 «     694794. ACFH
 STACK BA8 VOLUMETRIC FLOR AT STANDARD CONDITIONS	
 OSSTD « 17.647 * OS • PS • (1. - (8NO/100)) / (TS * 460.)
           17.647 t     694794. *  28.60 * (1. - (3.93/100))
 OS8TO » —.«....——.......—.—...———.——..—..—— •     611299. SCFH
	'	C—94. * 460.)	'			
 PERCENT ISOKINET1C
 ISO * (309.98* (T8»480.»l«t(0.002889«VLC)i'(VMT«(PB«(P*/13.6) )/TTM»460vn?/(TT«V8«P8«DN»DN)	
        (309.98*(  94,«460.))*((0.002669*  135.)*(  168.425*1.003*( 28.64*(   4.228/13.6))/(   78.4460.)))
                                    144. *     57.77 *   28.60 •  .258 *  .298
                                                                                                         •m 1M»>8 PtRgg*
 PARTICULATE LOADING — EPA METHOD 9 (AT STANDARD CONDITIONS)
 CS • 0.001  * MM * 19.41 / VMfTD
 ta a v.Owi  •    3i.4 • i5.43 /   160.494 *     .003 K«/i)8CC"
 PARTICULATE LB8/HR •• CPA METHOD -9
     « IS « U88TD / (19,43 t 893.6)
 PMR •     .003 *     611299. / (19.43 * 493.6)  •      .26

-------
FIELD  DATA
«•*»•""•' 	
1
hr
T ' - "**.
f
IO
1 1
II
11 ' ' ,
14
IB
FLEET1"1"' — •"•* "•'••'*? !'•'•»>.'
SAMPLING LOCATION
SAMPLE TYPE
OPERATOR
AMBIENT TEMP.(DEG.F)
BnH.pHBoA. {Ib»n«k) '
STATIC PRESS. (IN. H80)
FILTER NUMBER (8)
STACK INSIDE DIM. (IN)
PITOT TUBE COEFF.
THERM. NO.
"f PRESIUIIIE MUKCHESTEffl "
8ACHOU3E »1 OUTLET
' XEAO
SANDY
70.
HONI80M

.61
0002183
	 "' 38.
.62
129
LEAKABE " '"'."•'"^"ir.v*^ 	 ,vm
METER CALIB. FACTO* 1.003
READ ft RECORD DATA tVERY 7.0
!* TRAVERSE SAMPLE CLOCK 6A8 METER
,. POINT TIME TIME READIN6
21
". INIT
»-02
« JL B-05
„ U) B-06
11 * S»W
3.55
3.47


«.
4^
" " 4 .
4.
4.
4.
«.
"" '" 4.
4.
4.
:* 3.
2.
J •
3.
3.
3.
3.
	 3.
3.
3.
3.
3.


VV
55
75
75
bi
35
35
10
05
05
95
90
V5~
30
45
70
70
90
75
60
55
45
ar-
il!
92.
92.
93.
93.
94.
94.
94.
95.
r*.
95.
95.
93.
96.
96.
96.
96.
96V
97.
97.
97.
98.
	 98.

76. 78. 10. 5
79. 78. 18.0
81. 73. t3.0
84. 75. 12.5
80. 75. 12.5
83. 77. 11.0
85. 77. 11.0
86. " 77. 10.3
87. 77. 10.5
88. 78. 10.5
89. 79. 10.0
84. 81. 8.0
85. 60. 9.0
81. 80. 8.0
83. 60. 9.0
I Tt"lWt) !* MU9|tV.
86. 80. 9.
87. 81. 9.
" 89. 88. 10.
89. 82. 10.
90. 83. 9.
92. 83. 9. '
93. 83. 9.
~93. " 83. "9.0
"" ' IS. ' f*» Mil '
• *¥J
240.
260.
265.
263.
230.
•90.
263.
255.
265.
850.
330.
250;
275.
280.
.y.T
890.
850.
880;
830.
880.
850.
890.
280. --



58.
58.
62.
66.
53.
« :?" > • •• •
55.
58.
60.
60.
60.
6fc!
56.
60.
62.
62.
64.
68.
64.
65.
64.


"\










71
T«
79
'<¥

-------
           PARTICULATE FIELD DATA • RESULTS TABULATION



PLANT- NAME AND ADDRESS               TEST TEAM LEADER
> PRESTOLITE MANCHESTER* IONA
', TEST
I
to TEST
„ TB
„ ' T,F :
',', TT
.7 NP
,.'• """•"' y ' • •
z. ON

™
• PH '
1
lt^
Tw
i VMSTO
VLC
VNC
BNO
FMD
PCC2
P02
PCO
PN2
MD
HNS
B1L-1 BAGHOU8E *1 OUTLET

DATE
TIME-START
'" '•'• TIME*FINISH vw "•"!* »•.!>•'».•'•>'
NET TIME OF TEST, MIN.
NET SAMPLING POINTS
' METC* CALIBRATION riCTOr1
SAMPLING NOZILE DIAMETER
PITOT TUBE COEFFICIENT
1 AVER ABE ORIFICE PRESSURE'
DROP
VOLUME Of DRV CAS SAMPLED
AT METER CONDITIONS
VOLUME OF DRV CAS SAMPLED
AT STANDARD CONDITIONS*
TOTAL H20 COLLECTED IN

916 916 !!
T''"". 	 1351 	 • 	 <'•'""•"' H51 • • ' ' 	 .- ••' •""•''- ": ' r
196.0 196.0 i|*
28 28
*'"'•'"' """""' I, HUS " 	 - ^ VT--- 1 |.WWJ v. --. - - ,;«-.,.- I" . -< i ••" - -„
.258 IN 6.6 MM ['.
.82 .82
; • : !*
224.255 CU-Ff 6.350 CU-M 	 :,,
, 	 ' fl»f fc .',-•••• •;••', • • » ^ - -T1«l
213.047 8CF 6.033 SCM ;]
60.5 60.5
2.848 SCF .081 SCM ,'|
1.32 1.32
' ''"' ' .987 ' ' ' .987 '' '
.00 .00
20.90 20.90
.00 .00 "'»
28.84 28.84
28.69 28.69

-------
PB        BAROMETRIC PRESSURE



PSI       STATIC PRES OP STACK CAS
20.80  IN-HG



  .81  IN-H20
731.52



 20.57
MN-H6



MM-H20
PS STACK PRES» ABS.
20.66 IN-M8 733.03 NM-H8
tS AVERAGE StACK Ttrtp w, r 33. t
V8 AV6 STACK 6AS VELOCITY 57.0 FPS 17.4 MPS
AS STACK AREA
• ' -' ''
1142. 80-IN .737 80-M
DSSTU MACK FLOn RATE» DRT» mraiv*. SCFH *I7«« OC*H
08 ACTUAL STACK FLOW RATE 1627474. ACFH 46005. ACMH
ISO PERCENT IBOKtNETlC;
UN TOTAL' LEAD 	 ' i"1"
M6. EPA 5
PMR TOTAL LEAD
' " ' (.MISSION RATE "'
MN FILTERABLE 'PART.
^ C8 • > FlLTEIUSU fMT^l
L PMR FILTERABLE PART.
tn EMISSION RATE
• V68 DEO F» 'in^iz 1N7H8.



" ii.i ti;i ~
.169 LB/MR .08 KB/MR
25.3 25.3
j; 'L .0010 6R/D8CF* 4.194 M6/OBCM
.386 LB/MR .18 KB/MR
Tr"" ' '^ " "" "•'-*"" "" ' '"" **•**•"•*—•• -'•*<





*Y"-- . V . — M — , . ,...,..„

..... ^v,^.T-;v.r-—T; .. '-"..-ijifj), llp|p|| :|^apH^ ^-jjy?^ " •f'-r^'WK,--, ".'I,-!"- - <. ' *. - '.^ ... • •' -?' ' •, ".?1 '^«W* !•; v,.^.,.. ; • ' .,....,,. ^



""•'•" -'• ' ' ' "; >••- ""
t (•
/
«














;V

-------
                EXAMPLE  PARTICULATE CALCULATIONS TEST NO. B1L-1


                     BAGHOUSE  »\  OUTLET
7l	VOLUME  OF-pRTGAS  SAMPLED Tr STANDARD COWPITTON3~~	

         VMSTD » (17.647  •  VH •  T *  (PB + PM / 13.6))  / (TM * 460.)
                    17.647  *    224.295 * 1.003 * ( 28.60 * 3.907 / 13.6)
          VM8TD  «  »—••«»•»-••-•«»—»•••—————»•»•—•••••••••» •213.0*7 08CF
          VOLUME  OF  WATER  VAPOH AT STANDARD CONDITIONS

                       * vo:	*^~"—	
          VNC  «  .04707  *    61.  •   2.05 8CF
         PERCENT  MOI9TUKE  IN 8TACK  8A5


         BNO  •  (100.  *  VNC)  / (VMSTD » VNC)
                    100.  *    t«89
         BNO «———•—•—••••«-•-•—•• .•«  1.32 PERCENT
    "•*•               ZTT.VWf
    CTi
         MOLE  FRACTION  OF  DRY  STACK 6A8


         "FhD » (100.  •  BnO)/100.


                    100. •1.3
                        MMHM

                         100.
Fit- .r-"V •>-•?•-   .                   • r  • -p.
          AVERAGE  MOLECULAR HEIGHT OF DRY STACK GA8
         MD  •  (PC02  *  .44)  » <(»02 * .32) * (PN2 * PCO)  «.*•''"
              T  .00*44/100)  * 120.9*32/11X0)  '» ((79.14 .0)  »" 28/100 » ~  28.84'
          MOLECULAR  HEIGHT  OF  STACK GAS


          KWS  » HD * Ur^~tBHO/IOXU) '» 1^7 « (BNO/100)
   	MMS  •   28.84*  (1.  -(  1.32/100))  * 18. • ( 1.32/100)  »   28.6*

 L.		:__			

-------
 STACK GAS VELOCITY AT STACK CONDITIONS
 OELP • SUM. OF THE SQRTCVH * (T8 * 460.))
 VS • 89.49 * CP • DELP / (30RT(M*8 • PS) * PNTS)
      89.49 •—r8r-»—699.431 / CSOBTC as.69 » g»i8»r~•-*•- gg; »—sr.-o?
 STACK 8A8 VOLUMETRIC >LO« AT 8TACK CONDITIONS
 08 « f8 *-»y-
 OS •   37.02 •  1142. 3600/144 •    1627474. ACFH
                           AT
 OSSTO • 17.647 * 08 • PS * (1. • (8NO/100)) / (T8 * 460.)
           17,647 ft    1627474. •  28.66 •(!.-( 1.32/100))
 OS8TD « .—••»»«»•«*».»••-«»»•»•.«.»-»-—••••«•«•—.•••»»- «     1474194.  8CFM
                    (  !;:" *v •
 PERtKNT I80KINETIC
-ISO » (308.S8«CT8*480.))«ttO;002»6»iVLC)<'(VN»T«tP8»(P>l/t3.6ny(TM»4»fr;)n/(TT«V8«P8tO>««ON)
        (30S.58*(  99. *460.))*((0. 002669*   61.)«(  224.2S3*i;003*(  28.804(    3. 907/13. 6))/(  82.*460.)))
        mmmmmmmmmmmmmmmmmmmmmmmmmmmmmmmmmmmwmmmmm»mmm»mmmmmmmmmmmmmmmmmm,mmmmmmwmmmmmmmmmm,mmmmmmmmmwmmm .
                                    196. *     97.02 *   28.86 •   .ISO  *   .298
 PARTICULATE LOADIN6 •• EPA METHOD 9 (AT STANDARD CONDITIONS)
 CS » 0.001 • MN • 19.41 /VMSTO
 CS * 0.001 *    ll.l * 19.43 /   213.047 tt     .001
 PARTICULATE L88/MR *• IPA METHOD
 PUR « CS t U58TU / tti.43 t 893.6)
 PMR «     .001 *    1474194. / (19.43 * 493.6) »       .17

-------
FIELD  DATA



SAMPLIN8 LOCATION
SAMPLE TTPE
OPERATOR
AMBIENT TEMP.(DEG.F)
BAR. PRESS. I IN. HG)
STATIC PRESS. (IN. H20)
FILTER NUMBER(S)
STACK INSIDE DIM. (IN)
PITOT TUBE COEFF.
THERM. NO.
	 -PRETTOLI
BA6HOUSE
Tf, HA>
NO. 1
ICHETTir
OUTLET


" " CEAD/FILT.PART.
PROHASKA
85.
""• ZB.BB
.80
0001985
38.10
.80
128
- — inr






' LEAKASC " .ovv crw • a«w m»nv
METER CALIB. FACTOR 1.044
READ * RECORD DATA EVERT 7.0 MINUTES
TRAVERSE SAMPLE CLOCK 6AS METER VELOCITY
POINT TIME TIME READING HEAD
'.<"•?• ' .'.. • wov"
-
INIT
B-13
to 9~li
1 B-ll
£» B-10
00 B-09
6—06
B-07
8-06
	 B-05
B-04
8-03
8-01
A-13
A-13
A-12
A-ll
A-09
A-OB
A»07
A-06
A-05
A-03
A-02
A-OI
TOTALS

"•.<•• iPun.:.j«w»Hir ••*?"'*
CLOCK)
0 1450
14^0 1504
21.0 1511
£8.0 ' 1510
35.0 1525
42.0 1532
•:"' ' *9.0 ": ; |5JV." •••'"-y
56.0 1546
63.0 1553
	 70.0 ' 1600 '
77.0 1607
84.0 1614
9elo 1628
105.0 1651
112.0 ' 1658
119.0 1705
126.0 1712
14olo 1726
147.0 1733
"' 154.0 " 	 1740 	
161.0 1747
168.0 1754
182.0 1821
189.0 1828
196.0 1835
196.0

ICD.FT,'J 11
184.724
" 191.450 "-*"• ""
198.550
205.730
"2137000 — —
220.550
228.140
435»**vO *
243.700
251.720
"259.850
268.220
276.460
292^274
299.270
306.500
313.000
321.250
336I&00
344.300
"351.950
359.670
367.270
383.000
391.000
396.631
211.907

mnevj

.930
.950
.990
1.000
1.050
™ 1 . 1 v 0
1.100
1.150
1.200
1.300
1.250
1.100
.910
'.910
1.000
1.050
1.100
1.100
1.100
1.100
1.050
1.100
1.000
' .820

ORIFICE PRESSURE
DIFFERENTIAL
"""""" 1 1W.
DESIRED

'"•?'" 13.10
3.50
3.58
3.74
3.80
3.98
4.20
4.38
4.58
4.96
4.75
""•'.'" "-4* B)0
4.18
3.46
3.46
3.81
4.00
4.20
4.20
— — ».^o
4.20
4.00
4.20
3.80
"3.18
	 	 «;oi
fTCUl
ACTUAL

1 " j;zo
3.50
3.60
	 3.75"
3.80
4.00
4.20
4.40
4.60
4.95
4.75
4)20
3.45
3.45
3.80
4.00
4.20
4.20
~~ 4.20
4.20
4.00
4.00
4.20
3.80
" 3.20
....
STACK
TEMP
(DEG.F)

9s!
98.
98.
98.
98.
99.
99.
98.
97.
98.
" 98.
97.
97.
97.'
97.
97.
•
96.
97.
97. '
97.
96.
9*.
96.
96.
96.
97.
	 DATE 	
RUN NUMBER
PROBE LENGTH I TYPE
NOZZLE 1 1.0.
ASSUMED MOISTURE
" 	 " SAMPLE BOX NUMBER
METER BOX NUMBER
METER HEAD DIFF.
PROBE HEATER SETTING
HEATER BOX SETTING
K FACTOR
B1L-2
5 FOOT
.254
1.5
113
FIO
1.80
81.
250.
2151.5

GLASS



DRY GAS METER PUMP SAMPLE IMPINGER
TEMP VACUUM BOX TEMP TEMP


rr
1DEG.F) (IN«Wf) (DEH.FJ (OE6.P) ' 	 :•
INLET OUTLET

' 84. " ' •!•' ""' 't.O "
86. 83. 2.0
90. 84. 2.0
92. 85. 2.0
94. 86. 2.0
95. 87. 2.0
97. 88. 2.0
99. 90. 2.0
98. 91. 2.0
96. 90. 2.0
95. 90. 2.0
9B. 	 '•' '»li "" "'"t.O"
95. 90. 2.0
93. 90. 2.0
93. 91. 2.0
94. 91. 2.0
95. 91. 2.0
93. 91. 2.0
92. 91. 2.0
93. 91. 2.0
93. 91. 2.0
91. 90. i.O
90. 90. 2.0
90. 90. 2.0
93". 89; 2.0
'"93; ' 89. "••fiO


290.
300.
~2STO.
250.
250.
250.
300.
250.
300.
280.
*4«.
270.
310.
280.
270.
280.
300.
280.
230.
260.
• 90* •
250.
250.
250.
870.



90.
92. \l
50.
50.
52.
52.
52.
50.
52.
52.
•St. 	 - -P-
52.
58.
58,
60.
60.
60.
60.
62.
64.
6ft. • - T
60.
60.
60,
96. ' - • '"•'






-------
           PARTICULATE FIELD DATA I RESULTS TABULATION



PLANT* NAME AND ADDRESS               TEST TEAM LEADER
, PRESTOLITE* MANCHESTER PROHASKA
i TEST

10 TtM
,, TB
• > , ' TF
!l TT
" NP
'• " r; ?T
ON
.. , .....
CP
1
VM8TO
VLC
VNC
BNO
FMD
1
PC 02
P02
- •
PCO
PN2
MD
MN8
B1L-2 BABHOUSE NO* 1 OUTLET
'. -^-i-.. •••' ' ' ' ^
DATE
TIME-START
1 ' '**• \~\ "•
NET TIME OF TEST, Wt^fef; '
NET SAMPLING POINTS
SAMPLING NOZZLE DIAMETER
PITOT TUBE COEFFICIENT
<• •'• DROP - '' '.:'
WLunc ur u«i vna ounrueu
AT METER CONDITIONS
VOtUME OF DRY GAS SAMPLED
	 "' AT STANDARD CONDITIONS* 	 "
TOTAL M20 COLLECTED IN
VOLUME OF MATER VAPOR
' 	 	 AT STANDARD CONDITIONS* "
PERCENT MOISTURE BY VOLUME
' /,?'??.'• "•.; • - • ••• "•.,'. !-• '- '.•^r-'-'T"1 *wm
MOLE FRACTION DRY «AS
PERCENT C02 BY VOL.* 'DRY
PERCENT 02 BY VOL. » DRY
PERCENT CO BY ViulTlWY "
PERCENT N2 BY VOL.* DRY
MOLECULAR NT-DRY STACK 8AS
MOLECULAR NT-STACK GAS

ENGLISH UNITS
06/10/81
1450
146.0
28
' ' F«W*4^ *"""
.254 IN
.80
! Witts • tN"MIOT
Z11.40T CU"FT
VW F ."'; •"
206.694 SCF
13.0
•612 SCF
.30
.44t
	 i'OO 	
20.90
.00
28.84
2S.80


METRIC UNITS
06/10
1450
146.0
28
6.5
.80
.001
tf*
5.892
13.0
.•1?
.30

.00
20.90
.00
79.10
28.84
28.80
7OT
•- - i ':

-MM


CU"M





sen :;

SCM



.... #t ^ - - -^
J
" •







-------
PB BAROMETRIC PRESSURE
P8I STATIC PRES OF STACK GAS
1 PS STACK PRESf ABS.
' « • <•
4 fa AVERAGE afAck TIMP
. VS AV6 STACK CAS VELOCITY
. AS STACK AREA
.
10 B33TD STACK FLU* KAVEr Dfcf«
11 OS ACTUAL STACK FLON RATE
','. ISO PERCENT ISOKINETIC
IS ' ' ' i_
rMN TOTAL LEAD 	
M6. EPA 5
I", PMR TOTAL LEAD
»•*' 	 EMISSION RATE
» MN FILTERABLE PART.
I', CS FILTERABLE PART. .
,.' > PMR FILTERABLE PART.
,. 1 EMISSION RATE
11 ° * 6ft DEC F, 29.92 IN.H8.
13 .
34
39
J9
-40
4t
43 •• T:- - "-•'.' "^ rv'-- '. -•'• •'-••••• "• ' . •- I*-
44
41
SO *- ; '• •''
at
92
SI
94
S6
28.88 IN-H6 733.55 MM-H6
.80 JN-H20 20.32 MH-H20
28.94 IN-H6 735.05 MM-M6 '' ^
'"9TT ' f 	 """ *&• 	 "C " "" " " - - - — . - ...
57.3 FPS 17.5 MPS
1140. 80-IN .736 80"M
""" 1492908. StFH 42275. SCuH
1634072. ACFH 46272. ACMH
••' '' • ' "• * "" "! 	 ' ' / ».
95.3 95.3 '
"'
.131 LB/HR .06 K6/HR
14.8 14.8
.0011 6R/OSCF* 2.529 M6/D8CM
.236 LB/HR .11 KC/HR



.
'
'









24














-------
! •

 .
                 EXAMPLE PARTICIPATE CALCULATIONS  TEST NO. B1L-2


                      BAGHOU3E NO. t OUTLET
VOLUME OP  DRT CAS SAMPLED AT STANDARD  CONDITIONS	


VMSTO *  (17.647 • VM • Y * (PB » PM  /  13.6))  / (TM 4 460.)


           17,647 *   tit.907 • 1.044 • (  28.88 4 4.016 /  13.6)
VM8TD • .*.»•*»».••*»•.•-•«•••••••••».»».•-«—»..••—.—.•—— «     206.6S9 D8CP	
                          (91.'»  460.)~""'     	




VOLUMt OF  NATER VAPOR AT ITANOARO  CONDITIONS

VRC « »04707  • VLC	 i'k-ftfeflfc 	_	,—,	,	,	——	—


VNC • ,04707  •   13* •    .61 §CF	           	   		
                                   -                    -«-«-*•- . ••••••-VI-., -  •      " "- -    ^~!Xf7-^



PtRCEUT  MOISTURE IN STACK 8A8  '	—	  	


•MO • (100.0 VNC) / (VMSTO + VHC)   	         	                        	


  "•;";      10», • '" '»»i'V'   ."'\ j  >'•      '  *
9110 •*• '»**«B»«»*»*»««M»•»**•**•••**•*%***rti J9-  «30  FCnCCNT






MOLt FRACTION OF ORt STACK OAS f                             i

FWO fc(100.* BhO)/ 100.^___,.,,,,


           100.      .3                                           	___^__

                too*    •   •,     *v:!''
it
<>
14
»


I*
          AVERA0E  MOLECULAR NEI8MT Of  DRY  STACK CAS
          MO •  (PC02 * .44) * (POl *  .It)  * (PNI » PCD) • .21

          MU •  (	;t>OT44/100) » »0.f»»g/lOO)  » (I79.1»-^0? • 28/100
         	"-	'	>" .  .TO ^; i'-''^
          MOLECULAR NEIBHT or ITACK

         ~Miry t MO  * (i. * (BNO/loo)) -»  is.  «  (BNO/TOITT
          MNS «   28.84* (1, •(  .30/100))  *  IS.  * (  .30/100) •    28.80

-------
                                                                                                                                   o

    STACK  GAS VELOCITY AT STACK CONDITIONS
    DELP * SUM. OF THE 80RT(VH * (TS «• 460.))

    VS • 85.49 * CP * 0ELP / ISORTCMWS * PS) * PNT8)
          5iW"«  .80 *  67
                                                          «o. w
                                                          5 7. 33" TFT"
    STACK 6A8 VOLUMETRIC PLOH AT STACK CONDITIONS
    Off « VS * AS * S6UO/144"
    OS »   57.33 *  1140. 3600/144 •    1634072. ACFH
                              "-."'"f ^:'-'~T'
          6*8 VOLUMETRIC rLDR At BTATtOARD CONDITIONS	~~
    OSSTD • 17.647 • 08 * PS • (1. - (8MO/100)) / (TS 4 460.)
    088TD * ••
              17.6*7 *    1634079. *  28.94 * (I, - (  ,30/100))
                                                          1492908. 8CPH
                      T—97. + 460.)
    PERCENT ISOKINETIC  -
    lau
NJ
    1BW
(30S.S8*(  97«»460.))«( (0.002669*	*?•?**  f*!;^7***0***^2***6^	4,016/13.6) )/(   91.4460.)))
                            196. *     57.33 *   28.94 *  .254 *   .254
                                                                                                                      PIRCtNT
    PARTICULATE LOADIN6 — EPA METHOD 5 (AT STANDARD CONDITIONS)
                                                                                                                                         C
                                                                                                                                         c
    CS * 0.001  • MN * 1».43 / VM8TD
    C9  *  V.V01  *
                                                   ,001 ton/Dour
    PARTICULATE LB8/MR »• EPA METHOD S
                       (15.43 « <53.6)
PMR •
   .001 *
                        1492908. / (15.43 * 453.6) *
.IS

-------
FIELD  DATA
?•••-•' • ' ••-•• 	 '-••", • •" • • ~ •
> PLANT PRESTOLITE. MANCHESTER
» SAMPLING LOCATION BAGHOUSE NO. I OUTLET ,
• SAMPLE TYPE LEAO/FILT.PART.
• OPERATOR PROHASKA
DATE
RUN NUMBER
06/11/81
B1L-3
PROBE LENGTH A TYPE S FOOT GLASS
NOZZLE 4-1161 I.D. .254
,•'"'-. AMBIENT fEMP.(OeC.P) """ " 66. 	 ' ' " " ASSUMED MOISTURE 	 i.5 " " "
• , BAR. PRESS. (IN. HG) 26.96 SAMPLE BOX NUMBER 111
,, STATIC PRESS. (IN, H20) .00 METER BOX NUMBER F10
-o FILTER NUMBER (3) 0002240 METEH HEAD 01FF. i.BO
« STACK INSIDE DIM. (IN) 36.10 .00 ','.
• i PITOT TUBE COEFF. .BO PROBE HEATER SETTING 90. ..{
• >?*' * THERM. NO. *Wtl« HEATER BOX 8€TT1M« '"150. -
LEAKAGE , '•••*•*,* *<>00 CFM • 5.0 IN. MS
METER CALIB. FACTOR ^1, 044 K FACTOR 2112.3
" READ ft RECORD DATA {VERV 6.0 MINUTES
'. TRAVERSE SAMPLE CLOCK GAS METER VELOCITY ORIFICE PRESSURE STACK DRY GAS METER PUMP SAMPLE IMPINGER -.
*""•"'"' »6JMf ' TlNt TtMf W WA&lNB HtAb blfftirtNtUL TEMP TEMP ' VkCUl
NO. (MIN.) (Z«"MR (CU.FT.) UN.H20) (IN.H20) (DEG.F) (DEG.F) (IN.*

IPFTtOI HUP TfMP r ;; '
•6) (DEG.F) (OEG.F) !
DESIRED ACTUAL INLET OUTLET
:;
«@*,7-:••• 7^9f*T'^r^n\9t'599-^ - F '" ''•' " " •' * ' • •*>*•.•,• <*<" -r*-y.- - r~- »•- -i -.«}-,. • • . *• • ',.-
K:>"' -01 7.0 «OS 416.080 .020 3.23 3.25 91. 63. 62. . 3.0 290. 92.
A, -02 12.0 810, 421.090 .920 3.60 3.60 91. 71. 60. 3.0 250, 64.
u> -03 10.0 016 420.260 1.090 4.10
-04 24.0 B22 434.790 .090 4.14
-05 30.0 020 441.390 .050 4.16
ji.T-.T>fr".--rij-" .06 < .. B-12 156.0 1101 362.660 1.000 3.97
.10 92. 72. 64.
.15 92. 77. 66.
.15 93. 81. 68.
i40 93. 65. ^ 70. " T
.50 93. 87. 73.
.50 93. 88. 74.
.30 93. ~ "90. f6.
.30 93. 91. 77.
.15 93. 91. 60.
.10 94.' *' 'I. "^ •!• r **'
.65 94. 92. 61.
.60 94. 91. 62.
.95" 94. 90. 63.
.50 94. 89. 83.
.90 94. 90. 84.
.90 94. 91. 04,
.70 96. 86. 05.
.90 96. 89. 66.
.Tf 96. W. 15.
.55 96. 96. 67.
.35 97. 96. 88.
.13 v ' 97 i 9^. BY.
.15 97. 99. 40.
.00 97. 99. 91.
•i B-13 162.0 1107 589.170 .950 3.78 3.60 97. 100. 91.
B-14 168.0 1113 595.295 .660 3.50 3.50 96. 101. 92.
M
.0 260. 7o. ;
.0 260. 68. !
.0 270. 56. J
.0 2J7. •>' 34. ^ ^ •:* "**"
.0 270. 52. ;;'
.0 250. 52.
.0 ?40. 50. *"
.0 240. 52.
.0 250. 54.
»V ?6Q. "' 6U. '•'
.0 270. 52.
.0 260. 50. I
,
-------
PARTICIPATE FIELD DATA & RESULTS TABULATION
PLANT- NAME AND ADDRESS
PRESTOLITE, MANCHESTER
TEST

B1L-3 BA6HOUSE NO. 1 OUTLET
fiST TEAM LEADER
PROHA8KA

ENGLISH UNITS
TEST DATE
r TB
TF
TT
NP
V
ON
CP
PN*
> VM
1
*" TM
VMSTD
VLC
VMC
*?•'•• ••••- s*o
FMD
PCOZ
'• 4 POZ
PCO
PN2
MD
MHS
TIME-START
•TIME-FINISH
NET TIME OF TEST* MIN.
NET SAMPLING POINT?
METER CALIBRATION FACTOR
SAMPLING NOZZLE DIAMETER
PITOT TUBE COEFFICIENT
AVERAGE ORIFICE PRESSURE '
DROP
VOLUME OF DRV GAS SAMPLED
AT METER CONDITIONS
AVERAGE GAS METER TEMP
VOLUME OF DRV GAS SAMPLED
AT STANDARD CONDITIONS*
TOTAL H20 COLLECTED IN
IMPINGERS AND SILICA GELr*L
VOLUME OF NATER VAPOR
AT STANDARD CONDITIONS*
PERCENT MOISTURE BV VOLUME
MOLE FRACTION DRV GAS
PERCENT C02 BV VOL.* DRV
PERCENT 02 Bt VOL. > DRV
PERCENT CO BV VOL*, DRV
PERCENT NZ BV VOL.* DRV
MOLECULAR NT-ORV STACK GAB
MOLECULAR NT-STACK GAS
06/11/81
758
1113
166.0
28
1.044
.254 IN
.80
4.22 IN-M20
184.987 CU-FT
84.4 F
183.238 SCF
r»5.6 •• * '•'••
3.097 SCF
•f 1.66 "•- •'• - • •••-' '
.983
.00
ao.90
.00
79.10
28.64
28,66


METRIC U
06/11
T58
1113
168.0
28
1.044
6.5
.80
107.3
5.238
29.1
5.189
65.6
.066
1.66
.983
.00
£9*90
,00
79.10
26.64
28.66


NITS 	 ... _. _ 	 _ . . ,.__ . • _
/61



KM
NM-H20
CU-M
c
sen
•.•*:, t'/jf^" t\"-*\jt -; ,: • p""
sen
""" ""?"">"1 '*' ^"^^"
-------
 PB
BAROMETRIC PRESSURE
                                            28.96  IN-HG
  735.58  MM-HG
 MI       STATIC PRE8 OF STACK GAS

 PS 	STACK PRES, ABS.	

 TS        AVERAGE STACK TEMP
                                   .80  rS*H20

                                 29.02  IN-HG

                                 94.    F
   20.32

  737,08 ^NM-H6

   35.    C
          TVO stAtK 6*8 VELOCITY

           STACK AREA
                            	srvf	FTs~

                            	1140A_ ..SO-IN

                            1495144.    SCFH
   IT75   PPS

	.736 30-M

42338.    SCMH
                                                                                                                                   ~P1
 V8

. AS	

 QS3TO
           STACK FLOW RATE* ORV*
 08        ACTUAL STACK FLOW RATE

 IS0_	PERCENT ISOKtNETlC

 MN        TOTAL LEAD
	N8.EPA
 CS   ''     TOTAL LtAO
 PMR       TOTAL LEAD
             EMISSION RATE
    '.'' •••!?« FILTERABLE
    ,"•-    •  ,  US. EPA 5
"ts        FILTERA(§LE PlRT.

 PMR       FILTERABLE PART.
   _*__*•_ OKIBFr..
                            16458*3.

                            	*«*V

                                  T.3
46607.    ACMH

  _98,5   	

    7.3
                                   .0006 GR/OSCF*

                                   il32   L8/MR "
    1.415 PG/OSCP

       ,o~b  "KG/HR


                                 "^TOOI4 GR/OSCF *

                                   •29S   LB/HR
    3ii6i H'G/DSC»«

       .13   KG/HR
                                                                                                                         J
                                                                                                                                  	, j

-------
                 EXAMPLE PARTICULATE CALCULATIONS TEST NO. B1L-3
n
BA6MOUSE NO.  1  OUTLET
           VOLUME OF DRY GAS  SAMPLED AT STANDARD CONDITIONS

           VMST& • (17,64T~*  VM  • Y* (PB » PM /TsTtT)!" /  (TM + 46T.)                    "~

                     17..647 *	184,»87_* 1,044 *  ( 26,96  *  4.223 / 13,6)
           VMSTD »—————	————	............... •    183.238  DSCF
                                     (  84. * 460.)


      	VOLUME .OF JATER_^APQR >TJJ^JIAJO..CJ)J!!PIJIQN3 _   	   	

           VNC • .04707 * VLC

          VNC • .04707 *   6$7~i  TITO


           PERCENT MOISTURE IN STACK GAS                                                                                                          ,,|

         ^  BKO » CloTi * VWC) '7  (VM8TO * VWC)"T      "'      ""          '          ^~~~    ••>-'" •  '•- ' '  '    ?    'T^ ! '         """""''''
                    •
      	loo. •   J.t«   	    	  _	...   	.	    _    	  _____ _	
           BMO • .......................... •  1.66 PERCENT
       >              183.238 +    3.10


           MOLE. FRACTION OF_pRJf_STACK_6AS	

           PMD * (100. - BMO) /  100.






           AVERAGE MOLCCULAN  WCIOHT OF OR¥ STAtK GAB  	'^~'!  """  '^"   ^ "	"^       ~~~^   ' ^'r •"•.^--^•<   -?—-  --ST

           MD _» (PC02 *_,.44)  »_(^02_*_.»321 * (PN2_»_PCO) *. ,28		

           MO « (  .00*44/100) * (20.4*32/100) + ((79.1* .0)  * 28/100 *   28.84
                            •'.•..,,.•'                     '            •          '                  /-7rT~ 7^"   '""'','*," r: ,^ «™.~r

          .MOLECULAR HEIGHT OF. STACK. GAS ._ 	    _   	 	  	 . ._    	

           MMS * MD  * (1. -  (BMO/100)) * 18. * (BWO/100)
                                 ______^„-^-j-^--^ -t f;66/ijo) „   ia.66                     ""                   '
                                                                                                                                                  '*!

-------
   STACK 6*3 VELOCITY AT STACK CONDITIONS

   B«LP • 8uMrw~fMT~JoTTtvr«~tfi * uo.n	

   VS * 85.49 * CP * DELP / (SORT(MNS * PS)  * PNTS)
   VS > 85.49 *  .80 «  681.744 / (SORU 28.66 • 29.02)   *  28. •   57.75 FP3
_STACK 8AS VOIiUMtTMIC.PI.ON AT STACK CONDITIONS

   OS • VS * AS * 3600/144
"5f~i
*  1140.
                                              . ICfM
                         • _ • 	,  __ -j:.

   STACK CAS VOLUMETRIC FLOW AT STANDARD CONDITIONS



      	    17.647 » „  1645893. »  29.02 » (I. • ( 1.66/100))	
   (JiSTD » «-.-i---.—----—"--...—i———-•,—i——.— •    1495144. SCFH
                      (  94. * 460.)




  _f ERCMT ISOKINETIC ___	_.J		,			    ..	

   ISO • (305.S8*(TS*460.))*((0.0026»9*VLC)*(VM«V«(PB+(PM/13.6))/(TM+460.)))/(TT*VSKO«BO WWlTlgHtl     	  w  '•' " '""-"  •  «J--  "" ".W*.-'*.-1-.  ^ '»•;'>  ^!P^)" '"	

   CS « 0.001 • NN • 15.43 / VMSTD	,	

   CS » 0.001 *     7.3 * 15.43 /   183.238 m     .001 6R/03CF




   PARTICULATE LB8/HR «• EPA METHOD 5			 	   	

   PMR « CS * 0S8TD / (15.43 * 453.6)

        I	   ,Mi * "'••'

-------
FIELD  DATA
p?-"'- .'.' • . PLANT "" ~": ' '•»"•""•
89. 87. 9.0
91. 87. 9.0
"' ""' -^T
890.
290.
290. '


69.
70.
65.
65.
60.
65. r
60.
60.
55.
60.
60.
60.
60.
60.
60.
60.
64. . • • • - 4-^
60.
60.
•JO.
60.
65.
60.
60.
60.





,
|*|







-------
           PARTICULATE FIELD DATA • RESULTS TABULATION



PLANT- NAME AND ADDRESS               TEST TEAM LEADER
I PRESTOLITE, MANCHESTER PROHASKA
i TEST B1P-

10 ttsf DAIC
.1 TB
u TF
!! YT
!! NP
" ON
IX
CP
*-*
vo
VMSTO
VLC
VNC
BNO
FMD
PC02
P02
PCO
MD
MNS
1 BA6NOUSE NO 1 OUTLET
&>-'.; EN8LI8H UNITS METRIC UNITS °
i t
" ' " '"' Ob/10/81 06/10/81 ^^
T 4
TIME-START 1502 1502 1".
. / ' i"
NtY TIHE OF YMt, «!*» * 196.0 196.0 ''\ ",l
NET SAMPLING POINTS 28 28
4
nm nviwiiii iw-fwfyBjt*'!"'-''-->:vi :;i'*w*i * '-• •>• • i«**s f. ,».„... T r ;, . ,
SAMPLIN6 NOZZLE DIAMETER .258 IN 6.6 MM ',
PITOT TUBE COEFFICIENT .82 .82 •
x
DROP ; «
VbLU*£ of u(ti 6Av aAMPLED iSJt.il* tu-F t 6.boi CO-M >»
AT METER CONDITIONS ;;
<*
«w^""»^ W"^ »^^ » « ,1 . . t
VOLUME OF DRY OAS SAMPLED 218*891 SCF 6.198 SCM \
AT STAMbARD COwOH10H3« . , *
TOTAL H20 COLLECTED IN 58.1 58.1 ',
0
VOLUME OF MAYER VAPOR 2.735 SCF .OTT SCM f ',
AT STAtabARt) tOwdiliunS* >
PERCENT MOISTURE BY VOLUME 1.23 1.23 "t
MOLE FRACTION ORY 0A8 , .988 .988
4O
PCRCCHT CO** it VOL«f DHT 	 iOO .00 '
•t
PERCENT 02 BY VOL.* DRY 10.90 20.90 \
PERCENT CO BY VOL.* ORY ,00 .00 ;;
FtHCtMT M BT VOL.* OUT t^.iO t9.10 «•
MOLECULAR MT-ORV STACK 6AS 28.84 28.84 "
MOLECULAR NT*8TACK CAS 18. TO 28. to ',',

-------
PB
P3I
PS
" 	 TS"" 	 ""
V3
AS
OSSTD'
03
ISO
	 NN
• 	 ci ••? - : "'
PMR
MN
CS
1 PMR
(Tl
MN
CS
. FBR
	 MN 	 ' '
PMR
r ' •"
* 68



BAROMETRIC PRESSURE
STATIC PRES OP STACK GA3
STACK PRES, AB8.
AVERAGE STACK T£MK
AV6 STACK GAS VELOCITY
STACK AREA
STACK FLOH RATE* DHT*
ACTUAL STACK FLOW RATE
PERCENT ISOKINETIC
FILTERABLE PART
MG. EPA 5
FILTERAIll Pl»T™ n»|ww '^
FILTERABLE PART
EMISSION RATE
CONO. INORGANIC
CONO. INORGANIC
CONO. INORGANIC
EMISSION RATE
COND. ORGANIC
MG. EPA 5
CONO. ORGANIC
CQNU. UNBANIC
EMISSION RATE
TOTAL PBRtlCULAft
MG. EPA 5
TOTAL PARTICIPATE
EMISSION RAIt
OE6 F, 29.92 IN.HG.



28.88 IN-HG 733.55 KM-HC
.80 IN-H20 20.32 VM-H20
'!i«.".^ 	 -- v.- 	 ----. - : -• ' -~- 	 ' '.'•- ' ' •;. '" 	 |"r: '• '• " <~'i"^ t\
28.94 IN-HG' 735.05!KM-HS
TT. F J6. C
60.6 FPS 18.5 HP3
1140. 8B-IN .736 80-M
""• T564455. SCFH 44301. SCHH
1727994. ACFH 48932. ACMH
93.4 93.4
27.3 it. 3
JB ,..,, • ' ;0019 IR/BICPV "si;«M NV/DVOH 	 " •• W'""J ••"" 	 - 	 	 	
.430 LB/HR .20 KB/MR
1.7 1.7
.0001 GR/DSCP* .274 MG/DSCN
.027 LB/HR .01 K6/HR
3.1 3.1 !»
.0002 GR/D8CF* .500 MG/DSC*

32. i 32.1
.506 LB/HR .23 KG/HR ",

_



-------
                EXAMPLE PARTICIPATE CALCULATIONS TEST NO. B1P-1



                     BA6HOUSE NO 1 OUTLET
                                     °*;  w
          VOLUME OF OUT CAS SAMPLED AT STANDARD CONDITIONS	



          VMSTD • UT.M7 • VM • Y • •*•*•* ••**••»
          _Trr_fTr_f—j^	
PERCENT
          NOLC FKAfcTIOM OP WT STACK §AO
          PUD » (IOC. * BRUJ / 199.
          AVERAGE MOLECULAR HEIOUT OP DRY STACK CAS
4T



4*
|»i,
!»• "
          MO » (PC02 • .««) • tP02 ».,32) * (PN2 * PCO) * .28


          M0-«~t—,ooi«/ioo) » t»o;^«
-------
          STACK GAS VELOCITT AT STACK CONDITIONS

          DELP « SUM, OP THE SQRUVH *  (TS » 460.))                                                                     	        *"

          VS * 85.49 * CP * DELP / (SQRT(MNS * P8) * PNT8)    *^    .' *Mf
                        .82 *  697.895 /"tSfil»T(~?8.tO * 20V9T)«   ZTr"*1TDVS3
         —	—	'	";	'" :''"'-y—'	"" t '"  	'	'
          STACK 6A8 VOLUMETRIC FLOW AT 8TACK CONDITIONS
          OS »   60.63 *  1140. 3600/144 »     1727994. ACFH
          STXC"K"~CAS VOLUMETNlt ^LOH At

          OSSTD • 17.647 • OS • PS * (1. -  (BNO/100)) /  (TS •  460.)
                    17.647 *    1727994. •  28.94 *(!.-(  1.(3/100))
          P88TP « •—.»-...-.•.•.»..—...-.»»->————'•—<-'»——  •    1S644S5. 8CPM
              .j»?•
 PERCENT ISOKINETIC

T50 « (305.58*CT»*460.))«(C0.002669TVLCi*tVH*T»CPB»(PH/l3;g7rrCTTr^60.nT/tTT«V8"P8«DTil«DNT	

        (305.58*(  97.+460.))«((0.002669*   58.)»(   233.114*1.003*( 28.88+(   4.229/13.6))/(  90.+401.)))

                                    196. *
                                                        60.6B •    28.94  •   .258 *  .258
          PARTICULATE LOADIN6 « EPA METHOD S  (AT STANDARD CONDITIONS)
          CS * 0.001 * MN • IS.43 / VM8TD

                      	 27.3 rimr-T	218.891 •	;aOZ 6R/03CF
          PARTICULATE LB8/HR « EPA METHOD 5

73	PHH « CS » Q8STD / (18.43 » 453.6

          PMR «     .002 *    1564455. / (15.43 * 453.6) •       .43

-------
FIELD  DATA
[1 SAMPLING LOCATION
i
*7 	 	 ""SAMPLE TTPE
. OPERATOR
. AMBIENT TEMP. (DEB. F)
, ••" " "" BAR.PRKSS.UN.HBJ
, STATIC PRESS. (IN.H20)
. FILTER NUMBER (8)
,. STACK INSIDE DIM. UN)
PITOT TUBE COEFF.
.1 THERM. NO.
•f! rU- PWM IUL1
BA6HOUSE
LEAD
HOW I SON
70.
.75
4002251
37.75
.82
129
!•'.•« MCNT ' jy '. -'-r?r
»i OUTLET


.HO




U« IE
RUN NUMBER
PROBE LENB1
NOZZLE
ASSUMED M01
•H r-TYPT
t I.D.
STURE
8APPLE BUX NUMBER
METER BOX NUMBER
METER MEAD OIFF.
PROBE HEATER SETTING
HEATER BOX SETTING
B2L-1
-5 FOOT
.204
1.5
FB2
1.76
1.05
250.
250.
!! METER CALIB. FACTOR 1,003
READ • RECORD DATA EVER* 4.0 MINUTES
',", TRAVERSE SAMPLE CLOCK GAt METER VELOCITY
i. POINT TIME TIME READING HEAD
» *",'*' CLOCK)
at
» INIT 0 737
..yvv- *,.«• •-« •T'-Tjg J ;" ;j^^n
„ B-03 \ 18.0 819 >;
!!' 8-05 Solo 831
>. to B-06 36.0 837
', 8-08 48.0 849
„ B-09 54.0 655
,4 B-iu ou.g 4*1
,. B-ll 66.0 907
,. B-12 72.0 913
!.' B-14 8«Io 925
„ A-01 90.0 933
., A-02 46.0 4J4
A-03 102.0 945
„ A-04 108.0 1014
.4 A-06 120.0 1026
A-07 126.0 1032
„ 	 ' " A-08 132.9 igsa1""'*'"
„ A-09 138.0 1044
.. A-10 144.0 1050
4I "" 	 '" A*ll '' ' 15U.V"" 1999ft t^f
A-12 156.0 1192 ••••*
A- 13 162.0 1108
,, A-14 166.0 1114
!! TOTALS 168.0
nit
5 '

531.695
" 547.086
555.560
565!si5
570.975
*!'»97B.BSO "W
561.191
586.090
596^016
600.080
^ •05.842 "-'
410.618
614.680
624^174
626.763
638.472
643.395
"648.670 """
654.000
659.333
669.689
674.991
680.223
146.040


"taw
.300
.300
-1.250
.300
.350
* .190
.300
.200
.200
.200
.200
1 *150
.100
.900
.96*
.050
.050
1.150
1.200
17350
1.350
1.400
	 1.350
1.300
1.300
1.250

ORIFICE PRESSURE
DIFFERENTIAL
(In* nB9 f
DESIRED
6.00
2.18
2.10
2.18
2.27
'"'"""• "2 .10'
2.18
2.00
	 Z.tHT
2.00
2.00
.65
.50
177
.77
1.90
2.00
	 2;27-
2.27
2.35
2.16
2.18
2.10
..«
ACTUAL
5.40
2.18
2.10
2.16
2.27
' •*'. 4.10
2.18
2.00
' 2.00
2.00
2.00
, " 1.90
1.65
1.50
1.65
1.77
1.77
1.90
2.00
2.27
2.27
2.35
2.18
2.16
?.ro~
""'
STACK
TEMP
IBM.

" 4Tf
98
100
100
100
100
'"" 101
101
102
— ItI2
102
102
1UI
103
102
102
102
102
103
103
104
104
104
'.""104
104
104
~105
lot
r

«
.
.
.
.
.
.
.
.
•
.
.
.
.
.
•
.
.
.
.
.
*
.
.
•
.
.
.
DRY GAS METER
TEMP
I IDES .77
INLET OUTLET

64. 61.
70. 65.
75. "" 66.
79. 68.
83. 69.
1 "" "88. '-.'f'TI.)
89. 73.
92. 75.
93. 77;
94. 78.
94. 60.
95. 82.
93. 83.
' '"93." 	 ' 	 83.
94. 83.
95. 84.
91. 85.
95. 66.
98. 87.
100. 88.
102. 89.
102. "!' '90.
104. 92.
105. 93.
" T06; 94.
91. • 86.
81 ' " TJ
CLASS



PUMP SAMPLE IMPIN6ER
VACUUM BOX TEMP TEMP
il^^wr' cWEB.F I in
''*' W|f ••' ••
17.0
6.0
6.0
6.0
7.0
6.5
6.0
	 '6.0
6.0
6.0
5.5
4.5
5.0 '
5.0
5.0
5.5
6.9
6.5
6.5
7.0
'•••9
6.5
6.0
6.0

250*
259.
265. "
265.
265.
"ISOf '•'? ''•'
240.
250.
265.
240.
250.
249.
265.
255.
'2557 "
255.
255.
250.
240.
235.
260.
265.
265.
240.
260.
•9J.
VB.P] " " ' T

50.
50.
60.
50.
••50. '. • .- ' ;
50.
52.
54. -
56.
60.
_!_.• - - -in -irl
•64^ -: -- k,w-
66.
66.
66.
60.
60.
62.
62.
-~62;
65.
65.
-65, " !-'-' ff
66.
66.


)\













-------
           PARTICIPATE FIELD DATA S RESULTS TABULATION



PLANT- NAME AND ADDRESS               TEST TEAM LEADER
PRESTOLITE BATTERY
TEST

TtSf
T8
	 " 	 TF 	
TT
NP
ON
CP

J> VPI
P.HT |tn , .
VMSTD
VLC
VMC
BNO
FMO
PC02
P02
PCO
MD
MM8
B2L-1 BA6HOUSE *2 OUTLET

DATE
TIME-START
NET TIME OF TEST, MIN,
NET SAMPLING POINTS
SAMPLING NOZZLE DIAMETER
PITOT TUBE COEFFICIENT
DROP
VOLUME OF DRY GAS SAMPLED
AT METER CONDITIONS
""""'-","" AVER AGKfM METCM fBMP '" •'
VOLUME OF DRY GAS SAMPLED
' AT STANDARD CONDITIONS*
TOTAL H20 COLLECTED IN
IHP1NACM4 AM) SILICA ACLyMi,*
VOLUME OF NATER VAPOR
AT STANDARD CONDITIONS*
PERCENT MOISTURE BY VOLUME
MOLE FRACTION DRY GAB
PERCENT C02 BY VOL.* DRY
PERCENT 02 BY VOL.* DRV
PERCENT CO BY VOL.* DRV
(*tt*ttwt N2 BY VOL.* DRY
MOLECULAR NT-DRY STACK GAS
MOLECULAR XT-STACK 6AS
HOMI30N

ENGLISH UNITS
06/11/81
737
168.0
28
.204 IN
.82

146.040 CU— FT
• IT
138.467 SCF
47.6
2.241 SCF
1.59
.984
,00
20.90
.00
r9.ro
28.84
28.66
"

METRIC UNITS
06/11781 . . _
737
1114 ' ...... 	 	 .... . 	
168.0
28
"s.":" 1 .991 •' '" • 3 	 ' '"'• ' "W- vw* w !• . >-" - •- -- - - •- . '«••«",
3.2 MM
.82

4.133 CU»M
If, 3 C '- • "-!"'-! -; -. •iW-Vy-'-i •••••*• -it ?. ! •'••" •;"•• '"••* '•'
3.921 SCM
47.6
1 „ ' ' •''',• ' • ' *
.063 SCM
1.59
.984 ' .,,.,;,
20.90
.00
7v;lo
28.84
28.66












V

-------
PB BAROMETRIC PRESSURE
P8I STATIC PRES OF STACK
f- ••>• -f^:"., • • '•:\;'T9
PS STACK PRES, AB8.
29.03 IN-HB 737.36
6AS .79 IN-HZO 19.05
&.'v linpT*!^ ' ^?.7- • •• -;-*«!5rr- i 7 .
29.0« IN-HC ^ f 38.76
TS AVERA6C STACK TEMF iwe. t 51,
V8 AV6 STACK BA8 VELOCITY 63.9 FP8 19.4
AS ' '.STACK AREA '
' 1119* SO-IN .722
'j
o&std StAtK FLbM HA Til, BKV« is^rivi. SCFH , 45225.
08 ACTUAL STACK FLON RATE 1777142. ACFM 50323.
,..,,.. , i,^.,.^f, .,. •».',- •';--• . '.v.-,
ISO FERCENT ISOKtlttftC^
HN * ' TOTAL LEAD " '"T
M6. EPA S
PMR ' TOTAL LEAD
MN FILTERABLE FART.
*. ":'*;?" • '- *fl^j§S^*''''--:' *"» BF* * • -JWi^p'-MUJIi
^ Ci «/ 1vFlLTMABLt M»T»
01 FMR FILTERABLE FART*
EMISSION RATE
	 r^ot?^:«.*n^

* '•''•'••'••



ft •;..- - -•^•.^'-•-T-^v-'>1->*'-l^'!WfPMI*
•' *m>>!r, -
• •»?*•*«,'• • " ' ••***''* ' !«-; ~!<'*'- . >. '••
•'••£. 10*«0 106.0
><«-- *•* 2»4
' .060 LB/HR .03
12.2 12.2
^y$ A'f ^•Wf"" ' * %••• •'• "' "": :"- "•''' ' -' • -
,k ., • ,»OI4 BR/OSCF* 3.112
.310 LB/HR .14
^T^'" ^ r""

f^ ' "r" ":
'
^j^'^^-f^&^V''"-^'^-'' f,fir ;;;• s^*'"'- wr-.:--.

^PWP'*^1'"1 " "•'•" '" "* f;- ^ '-"" •'• '•
^
NM-HG
MM-H20 ^
.'MM-M6
FPS
10-M
ACMH
... ,- - .,- -r --/..-" - •-
i, i '
^

KC/HR

N6/D8CN
KC/HR
-. * ' -',^ W!'jl W ^P .-•--. — ."'• -Tf *;. • "r- v -f • -•--•.






•i.
. ...,,^,.,,,p... ,.r , ,- .. -
^,

1 0
1 1
14
*•
V
0
X
•
3
a
I
^
•
9
•
7
•
0
1
I
1
4j
7
a
t
i
4
t
«0
• 1
1
4
V
7
• t
TO
Tt
5
r

-------
                EXAMPLE PARTICIPATE CALCULATIONS TEST NO. B2L-1

                     BA6MOUSE «2 OUTLET
         -VOLUME OP OUT GAS SAMPLED AT STANDARD CONDITItmS	~

          VMSTD « (17.647 * VM * Y • (PB * PM / 13.6}) / (TM * 460.)
                    17.647 *   146.040 * 1.003 * ( 29.03 * 2.274 / 13.6)
          VMSTD • »«.•«»•—*.»»«••••••••••»».»•.«—»—.««•••«»••(••.— _•     136.467  08CP
                                   C85. » 460.)
          VOLUME OP HATER VAPOR AT STANDARD CONDITIONS
          VHC • *w«rvr •

          VNC • .04707 *   46. •   2.24 SCP
»c                            • -''

21
          PtkclNl nuiAIOkiL in STACK 6AS
"         BMO • (100. * VNC) / (VMSTD * VNC)
                    100. *   2*24
          BMO « •»•»»••.•.••»••»•-.•••*••» •  U8» PERCENT
       —.             136.461 v   2.24
          MOLE FRACTION OF DRY STACK SA8

          FMO » (100. • BMO) / 100.	
          AVERAGE MOLECULAR HEIGHT OF DRY STACK GAS
          MO » (PC02 * .44} • (POI * .32) * (PN2 * PCO) * .2S

          MO » I	,00»44/tOO) » (20.M3Z/100) » t(T9.1» .0) • ^8rt01> «	28,64
          MOLECULAR HEIGHT OF STACK 6A8

                                      * is. * (BNO/IOOI
          M»8 «  26.64* (1. -(1.59/100)) •» 16. * ( 1.89/100) •   ga*6fc  _ __ ....................... _   __  ______



         _________________ ' ______________________ _____ ____ _ _____ _._ _____ L _______________ _______ ______ .....  . ........ ____________ I

-------
                                                                                                                                     c> >
          STACK 6A8 VELOCITY AT STACK CONDITIONS
          OELP.« SUM. OP THE 8BRT(VH * (TS * 4*0.))
          VS • AS.4* • CP * DtlP / (SORTtMWS * PS) • PNT8)
                9;w «—.82 •—782,466 ?
          STACK 6AS VOLUMETRIC PLOD AT STACK CONDITIONS
          'W~» Vs~ • At
          08  •   63.91  *
                              , 1600/144 •    1777142. ACPH
tT
18
                                 N -v •*,„--? :,, :... ^|r^
-------
FIELD  DATA
/-r- — * 	 pr*in 	 	 	 ' — ' 	 • — — — PEEBTOLITE ""HimcHEBTeiu'iuwir • 	 • 	 - 	 DATE 	 VIMI/VI 	 • •• K
SAMPLING LOCATION BAGHOUSE *2 OUTLET RUN NUMBER B2L-2 •
L "' 	 " SAMPLE TYPE1 ' 	 LEAD " 	 ' PROBE LENGTH t TYPE 3 FOOT CLASS >
OPERATOR PROHA3KA NOZZLE 4-1161 I.D. .254 •
AMBIENT TEMP. (DEC. F) 80. ASSUMED MOISTURE 1.5 ,'
,~ BAH. PRESS. ( lh.h»») 29.03 • da^PLE 60» nUfcBEl 113 »
STATIC PRESS. ( IN. H20) .75 METER BOX NUMBER FB2
FILTER NUMBER(S) 0002128 METER HEAD DIFF. 1.76 ,
, ' STACK INSIDE DIM. UN) 37.75 .00 	 "n
, PITOT TUBE COEFF. .80 PROBE HEATER SETTING 250.
THERM. NO. 128 HEATER BOX SETTING 250. ;;
, '»""• 	 .'""" 	 "'"""LtAKABt ' "5'! •'" ' •.•-.""' - .004 CFM V S.t IN»MV '""" 	 '" "' . . .. ,. „ , . ,,.
METER CALIB. FACTOR 1.003 K FACTOR 2182.3
,, READ II RECORD DATA EVERY 6.0 MINUTES [I
" TRAVERSE SAMPLE CLOCK GAS METER VELOCITY ORIFICE PRESSURE STACK DRV GAS METER PUMP SAMPLE IMPIN6ER "
POINT TIME TIME READING HEAD DIFFERENTIAL TEMP TEMP_ VACUUM BOX TEMP ^ TEMP ['
11 *'."'" CLOCK)
21
.neyi un.ncu/ ivcb.p/ iuei».r» iin.i
DESIRED ACTUAL INLET OUTLET
17
10
" INIT 0 1216 681.869 j;
1 -02 • 12?0 1228 695.850 1*150 4.40 4.40 106. 99. 95.
-03 18.0 1234 703.270. 1.200 4.60 4.60 107. 102. 95.
,. \f -04 £4.v Ii40 710.950
' . -05 30.0 1246 718.080
S -06 36.0 1252 725.700
,! -08 48*0 1304 74U170
-09 54.0 1310 749.040
.4 -10 "' 60.0 1316 757.000
-11 66.0 1322 764.960
-12 72.0 1328 772.800
,, •»— u •*.•• ro.v »JJ"» •-•**•• • rou.vov
, A-14 84.0 1340 787.972
fl-01 90.0 1351 795.370
40 8*02 96.0 1357 802.920
B-03 102.0 1403 810.890
„ B-04 108.0 1409 818.870
'.' 8-06 120*0 1421 834.980
, B-07 126.0 1445 842.920
. B*08 '" 132. 0~" 1451 '" 	 850.900
B-09 138.0 1457 658.650
, 8-10 144.0 1503 866.350
',1 8-12 ISfclo 1515 88U300
8-13 162.0 1521 888.700
1.130 4.43 4.4? IVf, 1OB. fO.
.200 4.64 4.65 107. 109. 95.
.200 4.64 4.65 107. 110. 96.
.230 	 4.84 ' ' 4.83 109* ~ 110* 94. ' •>
.350 5.22 5.20 108. 111. 97.
.350 5.20 5.20 108. 112. 97.
.330 5.23 5.25 108. 113. 97.
.350 5.23 5.25 109. 114. 98.
.300 5.04 5.05 109. 114. 98.
.230 4.89 4.83 109* 114* '9V.
.200 4.64 4.65 109. 115. 98.
.150 4.46 4.45 108. 110. 100.
.250 ' 4.84 4.85 109. 111. 100.
.350 5.23 5.25 110. 114. 100.
.350 5.25 5.25 108. 115. 100.
*440 •; 3.46 « a**4 104. 116* 101* •
.400 3.46 5.45 108. 117. 101.
.350 5.21 5.20 108. 115. 101.
.350 3.20 ' 3.20 108. 107. 100.
.300 5.00 5.00 108. 107. 99.
.250 4.84 4.85 108. 109. 99.
• &00 4 Vfr3 4 • A3 i OS • ili* ^*»
.150 4.46 4.45 109. 111. 99.
.100 4.28 4.30 109. 111. 99.
To woT 7o! r<»
.0 260. 60. |;
.0 260; 60. ',,
.0 220. 60.
.0 230. 60. 4''
•9 ' ' 2M*1 '' ' >••« -" ' 	 "' 'i-'1!!"1
.0 230. 60.
.0 280. 60.
.0 260. 60.
.0 240. 60.
.9 260. 60. ^
.9 280, 60* ' ' '«
.3 240. 60.
.0 2so. 60. ;;
.3 230. - 60. ,j
.0 230. 60.
.0 240. 60. ;;
.0 • ~" 244*' "T '40. 7- - ; *'*, - 17
.0 230. 60.
.s 270. 60. ;;
.0 280. 60. it
.5 220. 60.
.5 280. 60. ;;
*v '•«*§ ' ••*• ' •'«»
.0 290. 60.
.0 240. 60.
„' B-14 168.0 1527 - 895.599 " 1.050 4.06 4.05 108. 111. VV. 4.0 iJOO. 60. -..
". TOTALS 168.0 213.730
'•• MVCNAbC . 4. 62 4.aj 144. 114* 96* 4*4 231* 40. "
« ' " ','

-------
           (•ARTICULATE FIELD DATA * RESULTS TABULATION



PLANT- NAME AND ADDRESS               TEST TEAM LEADER
fi f •• -
PRESTOLITE
"' H'T.v 'l^fPJWPJWf
* MANCHESTER* lOMA
T • ' .. t
PROHASKA
"!%r ' k - — ; ""'::'-• : ~ ' ~^F --— — - - -•- — ••— — 	 -- ----- - - p-,
TEST B2L-2 BA9HOUSE *l OUTLET

TEST DATE
TB
' " 	 TF - ^ 'H-
TT
NP
ON
CP
__^____^,___
1 ........
O> VM
vo
]', VM8TD
» VLC •
'! VNC
", BNO
FMD
44
44 PC02
» P02
" PCO
»> .
" Mb
MNS

TIME-START
NET TIME OF TE8T» Mt*V ' J" I
NET SAMPLING POINTS
SAMPLING NOZZLE DIAMETER
PITOT TUBE COEFFICIENT
DROP
VOLUME or1 DrtV GAS SAMfLCti
AT METER CONDITIONS
VOLUME OF DRY BAB SAMPLED
AT STANDARD CONDITIONS*
TOTAL H2Q COLLECTED IN
VOLUME OF NATER VAPOR
AT STANDARD CONDITIONS*
PERCENT MOISTURE BY VOLUME
MOLE FRACTION DRY BAS
PERCENT C02 Bt VOL.* DRY
PERCENT 02 BY VOL.* DRY
PERCENT CO BY VOL.* DRY
^itfCtwY ini oi VOL.* OrH
MOLECULAR NT-DRY STACK GAS
MOLECULAR NT-STACK BAB
ENGLISH UNITS
06/11/81
1216
T- 19IT''1" "Tlll!^4<:
16B.O
28
.294 IN
.80


196.999 SCF
94.8
2.979 SCF
1.29
.987
.00
20.90
.00
79. 10
28.84
28.70
METRIC UNITS
06/11/81
1216
168.0 ',
28 ;
6.9 'MM '
.80

6.052 CU-H
9.978 SCM
94.8
J^ .07J SCM _]
1.29
.987 ;
.00
(I
20.90
.00
	 T9.10 ~ 	 " '"" ' " " 	 " • • •
28.84
28.70 ;

-------
PB BAROMETRIC PRESSURE
PSI STATIC PRES OF STACK
";- - -'--. •- -.-,-• -,;: - - J .- (. '
PS STACK PRES, ABS.
29.03 IN-M6 737.36 KM-H6
GAS .75 IN-H20 19.05 MM»H20
• 	 - ' 	 -• - -.• '-: - - - 7- • • • ' 	 r ?\
29.09 IN-HG 738.76 MM-HG
T3 AVERAGE STACK TEMP ion. f *£• c
V3 AVG STACK 6AS VELOCITY 63.0 FPS 19.2 HP8
AS STACK AREA
	 • ••?» ••" • ' f -; -.- •'
1119. SO-IN .722 80-M
OSSTD STACK FLON HATE, URT« ISfUVflO, 3CPM 41*03. SCUM
i
QS ACTUAL STACK FLON RATE 1761458. ACFH 49879. ACMH
ISO PERCENT IBOKlNEtIC
< •'£
MN TOTAL LtAU
MG. EPA 5
CB •". ••; f uj AC U£AU v*^^:-f- ^*^
PMR TOTAL LEAD
EMISSION RATE
MN FILTERABLE PART*
'- v ' •-• > ; ' •: • MV« C*li?'»- '" ^ *? '/:v?-
'
C8 FILTERABLE PART*
1 PMR FILTERABLE PART.
Q EMISSION RATE
* 68 OE6 f, 29.92 1N.H0V
98.9 98.9
,;;. , f, ' ; '-'' '
".'" "*" ' ' 1*1 ii*t - - - ' -
.047 LB/HR .02 KG/MR \\
8.6 8.6
•0007 GR/08CF* 1.542 MG/08CM
.151 LB/HR .07 K6/HR
v-. •? , , ( • • - ' • V - .... -* ,|,

. ..,.,.,_,, , ., .„..., . . . .. r } , , . ^

• . - • - ;'.j.'.;* ;•• •'^*«' •:-. • '


•'-.„-.,-' ^ • • > ' .- ' "1 f • • - -15. • £ .
•

• • • . •'• '"-'••• '.--^'fff't «... • • ' • •••"• i^r... ', >*iKjS ' r\ . " •• ;.,
-

;

-------
                EXAMPLE PARTICIPATE CALCULATIONS TEST NO. B2L-2

                     BAOHOUSE *2 OUTLET
                    PRT CAS SAMPLED"*T STANDARD-CONDITIONS	

          VM9TD • (17.647 • VM • T • (PS * PM / 13.6))  /  (TM  *  460.)
                    17.647 *   213.730 « 1.003 *  ( 29.03 *  4.829  /  13.6)
          VMSTD » -—••*-•«•••—.—»-.•»-..—.-.•.-..—..«-.-.——.- «	i*.**A??_08C.'>
                                   r~104. * 4CT7)'      "
          VOLUME Of HATER VAPOR AT STANDARD CONDITIONS
          VWC • .04TB7 • VLC

          VNC « .04707 *   55. «   2.5* SCf
it         PERCENT MOISTURE IN 8)ACK S«S

          BNO • C100. * VNC) / (VMSTO * VNC)
                    100. *   2«S8
,7|         BNO • •<»•••-.«•••*••«»«»•»•—*•«.*» <•   1.29 PERCENT
    I

    -J
          MOLE FRACTION OF DRY STACK CAS

                      * BNO) / 100.	
          AVERAGE MOLECULAR NEI9HT OF DRV STACK CAS
          MO • (PC02 • .44) * (P02 •  .32) *  (PN2  «•  PCO)  *  ,2S

         "no » (  ;00«44/100) +  (20.1*32/100) '
          MOLECULAR NEI6MT OF STACK «A8

          MNS • 'MD * CTT""""
          MNS »  26.84* (1. •( 1.29/100)) *  16.  •  (  1.29/100)  •   28.70

-------
      STACK CAS VELOCITY AT STACK CONDITIONS
      DELP • SUM. Of THE SORT(VH *  (TS * 460.))
      VS • 85.49 « CP * DELP /  (80RT(MN8 * PS) * PNT8)   '
     ~V8-«-^5;49 »	.80 «	744.573 /  (SURT( gg.70 I 29.091	•—2»r~«	g2^95 FPS ~""	
      STACK GAS VOLUMETRIC PLOW AT STACK CONDITIONS
      08 l"V3" * AS t~1600/144	
      OS *   62.95 *  1119. 3600/144 •    1761458. ACFH
      STACK 6A8 VOLUMETRIC PtON AT 81 AWARD CUWD1TION8	
      OSSTD • 17.647 « OS * PS •  (1. -  (BNO/100)) / (TS * 460.)
                17.647 *    176145S. *  29.09 * (1. - ( 1.29/100))
      OSSTO • •••«•»••••«••••«.*•••«............................. •     1S70948.  SCPM
      PERCENT ISOKINETIC       '
" - 180
 to           (30S.S8*( 108. •460.))*((0. 002669*   53.)*(  213.730*1 ,003*( 29.03+(    4.829/13.6) )/(  104.4460.)))
                                         168. «     62.95 *   29.09 *   .254  •   .254
      PARTICIPATE LOADING — EPA METHOD 5 (AT STANDARD CONDITIONS)
      C8 • 0.001 * MN * It.43 / VMSTD
      CS « 0.001*2.7•i5.43 /
      P ARTICULATE LB8/HR •- EPA METHOD 5
     "P?lir~« C8 « U88TD 7 (15,43 • 453.6)
      PMR «     .000 •    1570948. / (15.43 « 453.6) •      .03


-------
FIELD  DATA
i ' "'•'•'• SAMPLING LOCATION ^^BAGMOUSE NO. 2 OUTLET
. SAMPLE YtPt Lfe**)/** tut. PART.
. OPERATOR PROHASKA
. AMBIENT TEMP.(OE6»F) 60.
[ STATIC PRESS. (IN.H20) !?S
. FILTER NUMBER (S) 0002131
,. 	 	 ' 	 "STACK INSIDE OIN.UNJ 	 37.75 .00
PITOT TUBE COEFF. .80
ti THERM. NO. 126
METER CALIB. PACTW , I. 003
READ • RECORD DATA IVCTf* *.».0 MINufES
sssspig? » -y • -S» " ' BATE ' "* '-.-••• vmritflll ' - ''4t'| IN
RUN NUMBER B2L-3 i |
	 PROBE LENGTH I TYPE 5 FOOT CLASS ~ ,
NOZZLE 4-1161 1.0. .254
ASSUMED MOISTURE 1.5 |
METER BOX NUMBER FB2 °
METER HEAD OIFF. 1.76
PROBE HEATER SETTING 65.
, HEATER BOX SETTING 250.
K FACTOR 2245.3 ;;
!" TRAVERSE SAMPLE CLOCK CAS METER VELOCITY ORIFICE PRESSURE STACK DRY CAS METER PUMP SAMPLE IMPINCER
.. POINT TIME TIME READING HEAD DIFFERENTIAL TEMP TEMP VACUUM BOX TEMP TEMP
i..^«**r, ••«-•• • no, •^-vi!«ii«»:T!f«^"iiwM^w^»yT-»*^T'?«w V r9c •sr^*^*'- V~ '" » 1 v • • * W • 1 yf «99 V
Z7 , B«03 .18.0 75e;*. t 917.950 1.400
1 '"• " "" B-04 lll"24. 0 804-""'" 925.770 '" l.*00 	
„ fr 8-05 30.0 810 933.700 1.400
1 8-06 36,0 816 941.700 1.400
'1 w B.Q6 48^0 ' 835» '»- 957.500 1*400
8-09 54.0 841 965.360 1.350
B-10 60.0 "* 847 ' 973.230 	 1.300
B-ll 66.0 853 960.610 1.200
B-12 72.0 659 986.300 1.150
"'""" '!" " "•• BM3 • 	 /8,W''"Vw 9V31!!*1 "' W995.TOW l«S'- '" 1.100 	
B-14 84.0 911 2.600 1.050
A-14 90.0 920 10.690 1.300
.0 	 ' »-13 96.0 	 926" 18.720 ~ 1.350 	
., -12 102.0 932 26.900 1.400
., -11 108.0 938 35.240 1.450
„„ ' ' ' -09 120.0 950 52.000 1.450
-06 126.0 1011 60.250 1.400
.,' -07 	 132.0 1017 	 68.100 ' 1.300
-06 136.0 1023 76.000 1.250
-05 ' 144.0 1029 83.700 1.200
i '..'"" ••••;.' ' ug« »T. 150,0 '«*" IVSl^'SVl'W'liOOO '"-"' IS WO »!•"•
-03 156.0 1041" 98.660 1.150
-02 162.0 1047 106.240 1.150
•
.20 5.20 97. 71. 63. 6.0 230. 34.
.42 5.40 99. 77. 65. 6.5 220. 65.
.45 5.4% 100. 82. 68. 6.5 25U. 64.
.50 5.50 100. 86. 70. 6.5 250. 61. "
.50 5. SO 100. 69. 72. 6.5 300. 59.
*,54 s!ss 10l! 91*, Tel 6.9 270. 52.
.35 5.35 101. 93. 79. 6.0 220. 55. j
^82
.62
.22
.26
r;46~
.67
.87
«|4» -* ^
.90
.64
.2*
.06
.87
.68
.70
„ " -01" '" 	 168.0 1033 113.156 .970 .94
TOTALS 168.0 217.209
i.20 101. ^B. BI. ».g J
-------
           PARTICULATE FIELD DATA t RESULTS TABULATION



PLANT- NAME AND ADDRESS               TEST TEAM LEADER
	 . 	 	 	 -
, PRE8TOLITE* MANCHESTER
TEST

TtSt
it TB
?••>«•' TF' •"
'", TT
NP
i« ' •'•' T '
ON
CP
>>
.j VM
• •• • i b • •••
VMSTD
VLC
VNC
BMO
.«.
FMO
pCui
P02
PCO
' ' PN2
MD
MWS
B2L-3 BAGHOU8E NO. 2 OUTLET

DATE
TIME-START
NET TIME OF TEST* MIN. XM
NET SAMPLING POINTS
•i. • ' MCTER 'C*Ll'RRI lURJ-'WWI'OlfT''
SAMPLING NOZZLE DIAMETER
PITOT TUBE COEFFICIENT
DROP ;1';5:
vuLUwt df OKI sAS iiAnHLcb
AT METER CONDITIONS
VOLUME OF DRY GAS SAMPLED
AT STANDARD CONDITIONS*
TOTAL H20 COLLECTED IN
VOLUME OF HATER VAPOR
At STANDARD tUNUl!jOn4«
PERCENT MOISTURE BY VOLUME
MOLE FRACTION DRY GAS
PERCENT 02 BY VOL.* DRY
PERCENT CO BY VOL.* DRY
~ PERCENT N2 BY VOL.* DRY
MOLECULAR MT-ORY STACK GAS
MOLECULAR MT*STACK GAS
PROHA8KA

ENGLISH UNITS
06/12/81
740
rr-v jojj i ••: •:>'»" f<
168.0
28
.254 IN
.80

217.709 CU-FT
204.260 8CF
73.5
3.460 8CF
1.67
.983
.00
20.90
.00
79.10
28.84
28.66
•

METRIC UNITS
Ob/12/01
740
U8.0 :
28
6.5 *M I;;
.80
'•"-V, '" '• 13V. 7 fWRIU • ' •: '• T"1* Sv'Hipi'1,^.'^ "'' - *W"W *9 ' '.'j.,11 '• •»1T!V1 .'. i "••'. i\< \iPf"lf!
6.151 CU-M ),
•
5.784 SCM ;;
73.5
' • *; . ' ' C?* " • .
.098 SCM ;;
1.67
.983
.00 ' 	 >i
20.90
.00 «•
" 	 79.10 ' ~ ' ' 	 j,.
28.84
28.66 ;•

-------
       PB        BAROMETRIC PRESSURE

       PSI       STATIC PRES OF STACK 6A3
                                  28.91   IN-HG

                                    .79   IN-H20
                          734.31   MM-HG

                           19.09   MM-H20
       PS

      TT

       VS
 STACK PRES, A8S.

 JVERHGF THICK"TCTP	

 AV6 STACK BA8 VELOCITY
       AS        STACK AREA

       UISTCr	STACK TLDN RATE; CRT*—

       OS        ACTUAL STACK FLOW RATE
      28.97   IN-H6         739.71   MM-M6

     101;     F              S8T~~ ~C

	63.6    FPS	    19.4    EPS	

    1119.    SO-IN             .722  80-M

"T99179T;     3tTH        *5T6TT;~"  "SCKff

 1780434.     ACFH        90417,     ACHH

     101.0                 101.0

                            y^


                            'i*»3  'pfc/oiCP

        .046	LB/MR	__»02  _KB/MR


       8.6	8.6


        .8006 6R/D8CF*	1.487  MS/08CN

        .148  LB/HR           .07   KB/HR
       ISO

      TNT"
 PERCENT ISOKINET1C
       PM1
 TOTAL LEllT"
   M6. EPA 9
 TOTAL LEAD
"~TMiniON RATE
       NN
 FILTERABLE PART.
'>  MS. EPA »  ' "r,

 FILTERABLE PANT.
                                                                                                                                               f
       C8
     1
    -J PMR
 FILTERABLE PANT.
   EMISSION RATE
          *  68 DEO F,   29.92 IN.HB.
&
b


-------
           EXAMPLE PARTICIPATE  CALCULATIONS TEST NO.  82L-3

                BA6HOU8E NO.2 OUTLET
     "UOCUHE OF DRT 8A8~8AMPLEO  AT STANDARD CONOTTttmS	

     VMSTD •  (17.647  •  VM  «  Y * (PB * PM / 13.6))  / (TM * 460.)
               17.647  *    217.20* * 1.003 * ( Z8.11  * 5.146 / 13.6)
     VMSTD « •••--•••--«••--•»•--»••*••-••-••«'•-••-••--••«••«•-•'•»-«204.260 08CF
     VOLUME OF HATER VAPOR  AT  STANDARD CONDITIONS
     VNC * .04707 • VLC

     VNC * .04707 *   74. •    3.46  8CF
     PERCENT HOI8TURE  IN STACK  6A8	
          V

     BNO • (100. • VNC) /  (VMSTO  *  VNC)
-J
               100. *   3*46
     BNO • ——-...»..-—.—»-—»-«••• :«   1. 67  PERCENT
     MOLE FRACTION OP DRY STACK OA8
     FHD »"t100. * BNO) /  100V
     AVERAGE MOLECULAR WEIGHT OP  DRY  STACK  GAS
     MO « (PC02 * .44) 4  (P02 *  .32)  *  (PN2  *  PCO)  •  .28

    "TO 1 (	.00*44/100)  •  (20.M32/100)  *  ((79rt*  .07  » T8/10O
     MOLECULAR NEI6NT OP STACK GAS
          ~HD * u. •  IDHO/1WU))" »  It.  •

     MN8 »  26.640  (l. -(  1.67/100))  »!».*(  1.67/100)  »    28.66
                                                                                                                                         "PI
                                                                                                                                          ',')

-------
      STACK 6AS VELOCITY AT STACK CONDITIONS

      OELP « SUM. Of THE 80RT(VH *  (TS + 460.))
 VS  *  S9.49 * CP * DELP / (SOP, t (HNS • PS) :* PNTS)

      19.49 *  .80 *  HO.511 / ISURTC ZB.fcfc « ZV\
                                                                2TT~«	1.3.S3 TP5
      STACK GAB VOLUPtWC PlOW AT STACK CONDITIONS

     "US » vs * AS
      03 »   63.63 •  1119. 3600/144 •     17S0434.  ACPH
                     -*-^

                                '"':' -^

            £*9 VtiLUMfcfMiC P'LUN At

      OSSTD * 17.647 * OS * PS  *  (1. •  (BNO/100))  /  (TS * 460.)
      flSSTD *
                17.M7
1710434. *
                                         *(!.-(  1.67/100))
                                                                   1S94794. 8CFH
                         T 101. * 460.)
JfeL
 I
 PERCENT ISOKINETIC

-rsmi
        (309.96*( J0i,»460.))•((*.002669*   74.)»(   217.209*1.003«( 2S.914(   9.146/13.6))/(   91.M60*)))
                                    in* »naaB>m»it>»********»»*****'*********Mi
                                    168. «     63.63 «    28.97  *  .294 •  .194
                                                                                                                  mit4 pent en T
      PAMTICULATE LOADIN6 ••  EPA  METHOD  9 (AT  STANDARD CONDITIONS)
 CS * 0.001 * MN * 19,43 / VMSTO

 CS * 0.001 *	?.7 * 19.43 /	Z1T47
                                                      .000 GR/DSCF
      PARTICUtATE LBS/MH »* |PA METHOD  9
 PMR •     .000 •    1994794. /  (19.43 • 493.6)  •
	r	?—yA;V.;  —:—'  .l'"l,-f^l."-:lll"'K—^~	'—T'—:—-4—r"T
                                                             .09

-------
FIELD  DATA
**•*»•.• * -

_

— . '» .; .'"!.» ( f " " V" '
PLANT
SAMPLING LOCATION
SAMPLE TYPE
OPERATOR
AMBIENT TEMP. (DEG.F)
BAR. PRESS. (IN. HG)
STATIC PRESS. (IN. H20)
FILTER NUM8ER(S)
STACK INSIDE DIM. (IN)
PITOT TUBE COEFF.
TXERM. NO.
LEAKAGE
METER CALIB. FACTOR
PRESTOLITE-MANCHESTER IA
BAGHOUSE *2
PARTICULATE
THOMAS
60.
26.91
.75
0662132
37.75
.62
-
.00
.000 CFM 8 4.0 IN.H6
1.044
<• READ « RECORD DATA EVERY 6.0 MINUTES
•• TRAVERSE SAMPLE CLOCK GAS METER VELOCITY ORII
,.t- r- POINT
NO.
'

' INIT
> 14
1 13
00 12
11
10
.-:•;- -•:.;"* 09
06
07
06
05
04
TIME ^ TIME1-"-"*"
(NIN.) 124-HR
CLOCK)


:*;•.• 0 •-."-. 742 ' '•'•*
6.0 746
12.0 754
18.0 600
24.0 606
30.0 812
'••.'•• 36.6 -"" 625 '•:>•?'*
42.0 631
48.0 637
"""•""54.6 	 843 	
60.0 649
66.0 855
03 72.0 901
02 76.0 906
! 01 84.0 912
1 90.0 922
96.0 926
•t 102.0 934
43 .'•
41
11
12
» 13
» 14
"l TOTALS
"•" AVERAGE
VL. ._ 	 _. ..
106.0 940
114.0 1010
120.0 1016
126.6 i022~~
132.0 1026
136.0 1034
144.0 1040
15.0 1046
156,0 1052
162.0 1058
168.0 1104
166.0
READING HEAD D
(CU.FT.) (IN.H20)


DATE
RUN NUMBER
PROBE LENGTH 1 TYPE
NOZZLE 4-122: I.D.
ASSUMED MOISTURE
SAMPLE BOX NUMBER
METER BOX NUMBER
06/12/61
B2P-1
5 FT GLASS
.258
t.5
109
F10

V MEUH HEAD OIFF. 1.80
PROBE HEATER SETTING 250.

rICE PRESSURE
rFFEUENflAC™
(IN.H20)
DESIRED

595.992
603.362 1
610.785
616.553
626.396
633.915
r»41.915
649.863
657.568
665.023
672.407
679.791
"667.665 "'""
694.314
701.048
707.943 ~
715.283
722.958
"730.641 ' "
738.372
746.141
""753.920
761.652
769.829
'777.790
765.658
793.530
801.270
806.716
1.300
.300
.400
.400
.400
.400
.400
.300
.200
.200
.150
.100
.100
.960
.000
.150
.300
-,3oo — r-i
.300
.300
.300
.350
.350
[.""350
.300 !
,300 '
.60
.50
.10
.10
.10
".20"
.20
.70
.30
.30
.20
.96
.00
.30
.50
.20
.90
.90
.90
.62
.85
.09
,09
.11
5.90
.250 5.68
.150 5.22
218.363
5.63
ACTUAL

9.60
5.65
6.10
6.16
6.10
—— 6-7?0-
6.20
5.70
5.30
5.30
5.20
4.90
5.00
4.30
4.50
5.20
5.90
5*,90
5.82
5.85
6.09
6.09
6.11
5.90
5,91
5.68
5.22
5.63

STACK
t€FP
(DEG.F)


95.
96*
99.
101.
166.
100.
100.
101."
lot.
100.
101.
101.
101.
101.
102.
102. 	
101.
104.
103.
104.
104.
104.
104.
105.
105.
101.
HEATER BOX SETTING
K FACTOR
DRY GAS METER PUMP
TEMP VACUUM'
(DEG.F) (IN.HG)
INLET OUTLET

66. 64. 2.0
63. 56. 2.0
80. 66. 2.0
85. 70. 2.0
89. 73. 2.0
89. • -*• '77. •" *t"9,9'
66. 80. 2.0
90. 60. 2.0
92. " " 82. " 2.0
94. 84. .5
97. 87. .5
100. 66. .5
102. 90. .5
104. 92. .0
103. 92. .0
102. 92. .0
104. 94. 2.0
lOl! 95! 2*.0
97. 95. 2.0
jofl. " 15. " ~~2~70"
104. 95. 3.0
106. 96. 3.0
106. 96. 3.0
109. 98. 3.0
110. 98. 3.0
110. 99. 3.0
110. 100. 3.0
97. 87. 2.1
256,
2507.
SAMPLE
IBS TEMP '
(DEG.F)


260.
250.
260.
270.
260.
260.
300.
280.
260.
265.
270.
265.
280.
"300.
260.
300.
270.
245.
245.
~245~.
250.
250.
270.
265.
260.
270.
270.
270.
5
IMPINGER
TEMP
(OEG.F)


55.
60.
60.
60.
60.
60. ' • ' '• ' ' " "*
65.
60. """ 	 "
60.
60.
60.
60.
60.
'"""55. 	
50.
60.
- 5H. 7 , -
56.
60.
65.
65.
60.
' 60.
62.
62.
68.
60.

7 t.
_
2
i <
12
,,
1
i 1
44
4 >!
4 8
5 '
*. ?
38
•- «;
ft 7
A 1
H
H
i
2
4

-------
PARTICULAR FIELD DATA * RESULTS TABULATION
PLANT* NAME AND ADDRESS
PRESTOLITE-MANCHESTER I*
TEST
B2P-1 BAGHOUSE «2
YlSt TEAM LEAOlR
THOMAS



1 ENGLISH UNITS METRIC UNITS i*
TEST
~ ' TG
TF
TT
NP
Y
DN
CP
PM
. b>
1
5 w
- i- - "* \ -f
TM
VMSTD
V4.C *
I
VNC
!.*" *•"' BNO
FMO
PC02
.-.:*,- *0* J
PCD
PN2
MD
MMS
DATE
.tI«t»«TAI»T - T
TIME-FINISH
NET TIME OF TEST, MIN.
NET SAMPLING POINTS
METER CALIBRATION FACTOR
SAMPLING NOZZLE DIAMETER
PITOT TUBE, COEFFICIENT ^
AVERAGE ORIFICE PRESSURE
. DROP
VOLUME OF DRY GAS SAMPLED
AT METER CONDITIONS
AVER ACE CAS METER TEMP
VOLUME OF DRY GAS SAMPLED
AT STANDARD CONDITIONS*
TOTAL M20 COLLECTED IN
IMPIN6ERS AND SILICA CELtML.
VOLUME OF NATER VAPOR
AT STANDARD CONDITIONS*
"' PERCENT MOISTUW «T VOLUME
MOLE FRACTION DRY CAS
PERCENT C02 BY VOL.. DRY
•" PERCENT 0* W m»» «V
PERCENT CO BY VOL., DRY
PERCENT N2 BY VOL.* DRY
MOLtCULA* Nt-DRV IfACK CAS
MOLECULAR NT-STACK GAS
06/12/81 06/12/81 ',
1
1104 1104
166.0 168.0
28 28
-•, • I- •-•. -.-j":-7— 'T ' ' r
1.044 - 1.044
.258 IN 6.6
.82 .62
... ( -.,, ^ . .
5.63 IN-H20 143.1
212.363 CU-FT 6.013
»1.7 V 33.2
207.958 SCF 5.669
«Vft -•'! -y T '•• 89.2
4.199 SCF .119
«980 _i_ ,980
.00 .00
_jLpO ,00
79.10 79.10
28.84 tl.84
28,62 28,62
" _
* -4
"''1
PW
• o
• i
3?
MM-H20 ]'
J 7
CU-M "
0
c ' ;
sen ;
'
, „ „,„..,.,, ., ,.. .. ,„ .., ...... .
:
3Cr« ^
-F
Ft
• 1
• 4
-,, .- , ;j
ft
70
J*
; *,

-------
PB
r r PSI
	 PS 	
TS ,
V8
AS
1
< 08STO
1
< 08
" ISO
16
" MN
!•
it •' '
»« CS
^ PNR
3
• 4
.» ' '• MN ' '
2«
17
KT~«
" 00
« 0 PMR
si ~" '
3
3_[ MN
3
3
CS
PMR
3 !
4
MN
•
4 f ^
. cs
4
« PMR
4
«•
MN
BO
B1
» CS
•>
B. PMR
BB
• 6
y 	 . MN
BAROMETRIC PRESSURE
STATIC PP.ES HP STACK "S*S~
STACK PRE8,ABS. 	
AVERA6E STACK TEMP
AV6 STACK CAS VELOCITY
STACK AREA
STACK FLO* RATE, DRV*
ACTUAL STACK FLOW tATE
PERCENT ISOKINET1C
FILTERABLE LEAD
MG. EPA 5
FILTERABLE LEAD
FILTERABLE LEAD
EMISSION RATE
CONO. LEAD
MS. EPA 5
CONO. LEAD
COND. LEAD
EMISSION KATE
FILTERABLE PART.
M6. EPA 5
FILTERABLE PART.
FILTERABLE PART.
EMISSION RATE
COND. INORGANIC
MG. EPA 5
COND. INORGANIC
COND. INORGANIC
EMISSION RATE
COND. ORGANIC
MG. EPA 5
COND. ORGANIC
CONO. ORGANIC
EMISSION RATE
TOTAL PARTICULATE
£8.91 IN-HG
	 .7* IN-H20
	 28. 97 IN-HO 	
101. F
M.t FPS
1119. SQ-IN
161586Z. SCFH
1010530. ACFM
98.4
3.1
.0002 GR/D8CF*
.053 LB/HR
.1 , ••
*
.0000 GR/DSCF*
.002 LB/HR
19.5
.0014 GR/DSCF*
.334 LB/HR
3.8
.0003 GR/D8CF*
365 LB"/HR
3.Z
.OOOZ GR/DSCF*
.055 LB/HR
Z6.5 	 	 	 	
734.31
19.05
735.71
39.
t«.T
.722
45756.
51269.
98.4
3.1
.530
.02
.1
<
.024
.00
19.5
3.312
.15
3.8
.645
.03
3.2
.543
.02
«fc.V
PM-HG
MM-H«d •.-•••• • ••.' - • -^:-i • --•••: -
HM-HG 	 _ 	 	 	 	 	 ._.._._ 	
C
MP8 • '
SO-M
SCMH
ACMH ",' ': ' • v" *'

MG/D3CN
KG/MR
f f ,, t ' •'• " - :" . . , '
KG/DSC"
KG/HR
'• > f :f"* '-i- '{. - ^ •*';.> " .V - ' - Hfl
MG/03CP
KG/HR

CG/DSC*1 •
KG/HR 	 "
,r , '.•>,•• ".T' ' - -. - • ' " - -- /
HG/DSCK
KG/HR
f ~ " ':. ^

f?
4
•t
•
i 0
1 4
1 P
'"
i i:
' 7t
.- 4
• n
• 4
1O>
1 1
11
il:
1 "i
7
1
•* 4
*v
« '
4|
t»
•\ '>
•> ' :
'i 2
9 •»
5*
S"i
t •!
1 '•
4 f>
* 2
« 1
A*
'>B
••«
61
«*
ro
7 i
7 t
3
MG. EPA 5

-------
ca
       JTJllAJL^A.fUJLCJMJLJEL.
PMR        TOTAL  PARTICULAR
	EMISSION RATE._
^0020 GR/DaCf«       4.501  I"6/D9CK.

 ,«54   LB/MR           .21   K6/HR
*  66 DEC
                         IN.H6.
                     ;•>>;  iT™1^..,
                                                                                                                                      	i
                                                                                                                                                 I

-------
                 EXAMPLE  PARTICIPATE CALCULATIONS TEST NO. B2P-1
    VOLUME  OF  DRV  GAS SAMPLED AT STANDARD CONDITIONS

   "VMSTD * uTTfciT"*



   ~VMsT6 •
           * Y • (PB » PM / 13.6)) y IfM » 140.)


17.647.*..„ 212.363 *_1,044._* (_28,91 .»_•


               (  92. » 460.)
                                                                              207.958  03CF
          .VOLUME Of KATE*  VAPOR AT STANDARD CONDITIONS


          VNC • .04797  * VLC
          VWC «  .04707  *-
          PERCENT MOISTURE  IN STACK GAS
          •«ro •  (IPO.  *  VNCJ  r (VMSTD * VNCI
                     I oo ;,_
    oo
    ro
          BNO
               207.998 *   4.20
                                     *  1.98 PERCENT
          FMD  •  (100.  -  BNO)  / 100.
          FMO • -•••
                     100.  *
                          ioo«.
                                      .9*0
                                    W^W


          MD •  (PC02  •  .44)  * (P02 *  ,32) * (PN2 * PCO) •_ t28	


          MD •  (   .00*44/100) «  (20*9*32/100)  • ((79.1» .0)  * 28/100 •   28.84
11

11
__MQLECULAR  HEIGHT OF 3TACR_G_AS	


   MM8  •  MD * (1.  • (BNO/100)) * 18. * (BMO/100)
MUS *  28.64* (1*
           1.98/100))
                                      18. * ( 1. 98/100) *
                                                                     . 6f

-------
           STACK  GAS VELOCITY AT STACK CONDITIONS
           DELP » SUM. Of THf JtalTCV* * (TS * 4*0.))

           VS..«. 85.49 * CP_J» OELP / (SflRTCMNS • PS) AJ'NTS)-	     	

           VS * 65.49 «  .02 •  744.141 / (SORT( 28.62 • 28.97)   •  28.  «    64.71 FPS
          .STACK, 6A8 _VQLUMTRlC_FLQ!LJIl_3TACK_COND_lT.JQNS_

           03 » VS * AS * 3600/144
08*   64«7i •*  1119*  36*1/144
                                                        ACPM

           STACK CAS VOlUMCTftIC PLOW AT STANDARD CONDITIONS
OS8TO * 1T.647 « II * P8
                                            tBNO/109)) ?  (Til  *  469.)
J
08STD
                              ( 101. * 4*0.)
                                                                             1615862. 8CFH
          J»E8C£MT.,I80HIH6I1C
     co    ISO » (305.58*(TS*460.))«C(0.0026*9*VLC)*(VM«r*(PB»(PN/13.6))/(TM*«60.)))/(TT*V9*P9»DN«ON)
     U)
                                                                                                                                                 l«
       (309*58*t  191. 4460.
ISO * ——.———.—.^
                                                                                                                     •  98.40 PERCENT
                                    1*B._.«L
                                                                   ..Z8.97 • . .258 *   .258
           PARTICULATE LOADTlW ** P* NefHWllIT ltti»IO**0 COIIOlf fO«S)

           CS « 0.001 * HN • 15.43 / VM8TQ	.		

           CS « 0.001 *     3.1 * 15.43 /    207.958 •      .000 GR/DSCF
          .PARTICULAR J.BS/MR»r_EPA_Mf;THOD 5	

           PMR • C8 • QSSTO / (15.43 * 453.6)

                           	 1*1586*; /  (15.43  *  448.6)

-------
FIELD DATA




•:: >•:••
PLANT
SAMPLING LOCATION
SAMPLE TYPE
OPERATOR
AMBIENT TEMP. (DEG.F)
BAR. PRESS. (IN. HG)
STATIC PRESS. (IN.H20)
FILTER NUMBER(S)
STACK INSIDE DIM. (IN)
PITOT TUBE COEFF.
THERM. NO.
LEAKAGE
METER CALIB. FACTOR
PRE3TOLITE, MANCHESTER* IONA
BAGHOUSE NO* 3 OUTLET
LEAD
DAN FITZGERALD
70.
26.60
-.62
•0002164
36.13 .00
.81
• 1*4
.004 CFM a 7
1.016
READ ft RECORD DATA EVERY 4.5 MINUTES
TRAVERSE SAMPLE CLOCK 6AS METER VELOCITY
|r~w". ' POINT v TIME TIME '"'••'-
NO. (MIN.) (24-HR
CLOCK)


READING HEAD
(CU.FT.) (IN.H20)




.0 IN.HG
ORIFICE PRESSURE




STACK
DIFFERENTIAL TEMP
(IN.H20) (DEG.F)
DESIRED ACTUAL

DATE 06/09/81
RUN NUMBER B3L-1
PROBE LENGTH S TYPE 5 FOOT GLASS
NOZZLE 4-102: I.D. .250
ASSUMED MOISTURE 2.0
SACPLE BOX NUMBER 111
METER BOX NUMBER FB3
METtH HEAD 01FF. 1.94
PROBE HEATER SETTING 250.
MEATtR BO* SETflNG * 2SO.
K FUCTOR C407.2
DRY 6A« METER PUMP SAMPLE IMPINGER
TE»*P VACUUM BOX TfcMP TEMP
(DEG.F) (IN.HG) (DEG.F) (DEG.F)
INLET OUTLET

INIT
IP B-OI
1 8-02
00 B-03
*> B-04
B-05
B-06
8-07
6-08
B-09
B-10
B-ll
B-12
B-13
8-14
A-01
TOTALS
AVERAGE
~ •• 9 i«ia """
4.5 1416
9.0 1443
13.5 1444
18.0 1452
22.5 1456
27.0 1501 r
31.5 1505
36.0 1510
40.5 1514
45.0 1519
49.5 1523
54.0 1528
56.5 1532
63.0 1537
67.5 1544
67.5

478.134 '
483.250 .000
468.615 ,400
494.905 .550
501.150 .600
507.455 .650

-------
PARTICULATE PIELO DATA • RESULTS TABULATION
1

PLANT* NAME AND ADDRlSt f
RBEI.TOtlT.Ei. MANCHESTER*. I.O.M 	 	
TE$T B3L-1 BAGMOUSE NO* 3 OUTLET

,' . " ' '
TEST DATE
F - ' '


f • l»*£4>
1
fW



	
'

TF
TT
NP
Y
ON
>!**P
I»M :'••'
VM
TM
VM8TD
vte •'••••
VNC
PMD
PC02
P02 "
PCO.
PN2
MO
MNS
' TlME-SfMT :-fy fi^"-:T'
TIME-FINISH ' . rv,^,.
NET TIME OF TEST* MIN.
NET SAMPLING POINTS
-">$><• . v .^.wwm^f.
METER CALIBRATION FACTOR
SAMPLING NOZZLE DIAMETER
PITOT TUBE COEFFICIENT
AVERAGE ORIFICE PRESSURE
. DROP , 	 	
VOLUME OF DRY GAS SAMPLED
AT METER CONDITIONS
. ..' . ' • • • . • •• *'*••' '••;•
AVERAGE GAS MITER TEMP
VOLUME OF DRY GAS SAMPLED
AT STANDARD CONDITIONS*
TOTAL H20 COUECTED IN
IMPINGERS AND SILICA GEL » ML
VOLUME OF MATER VAPOR
AT STANDARD CONDITIONS*
w PERCENT MOISTURE §Y muftjr
MOLE FRACTION DRY GAS
PERCENT C02 BY VOL»» DRV
PERCENT 0* -8r.-¥tUi"fO»t
PERCEMTJCLCLBy VOL.*. DRY
PERCENT N2 BY VOL.. DRV
MOLECULAR MT-ORY STACK GAS
MOLECULAR *»T«STACK GAS
TEST TEAM LEADER
DAN FITCGERAUD

1 \
[
.
ENGLISH UNITS METRIC UNITS ( '
06/09/81 06/09/81 "
1«M Mil
15«« 1544
67.5 67.5
1^ 15
1.018 1.018
.850 IN 6.4
.81 .81
Hf f?!!|! " ^-- - ' ,.-.,-., ^*-
•.41 IN-H20 1*2.9
89.468 CU-FT 2.533
f-J- jTi; -1 "?• (T -"**'' - ' *" • "••
74.1 F 23.4
87.485 SCF 2.477
•
1.850 SCF .052
V ' ^t« ttf '"""*' .-7T'-^-<" f.Ot
.00 .00
•'•• i«Y*;0 '•" "?"?•* '"to.**
*00 tOQ
79.10 79.10
28.84 88.84
20.61 28.61


] 7
MM "
t
MM-H20 '
CU-M "
C ' ': '!
SCM ;
i
i '
3CM
t 4
H
•
«
'
" •• T '. •• r <3!g>  ',-."' jf? •' . •
"•'. ' f
t
n
	 T; • 7 .--"-•; '•••«•. •..--• -,-.,--.- --- . . .. --.,-,...,,
T 4
T"

-------
PB
BAROMETRIC PRESSURE
                                           28.60  IN-HG
726.44  HM-HG
PS
TS
VS
AS
11 OSSTD
If
14
» ISO
I*
' MN
1*
> CS
2
' PMR
i
to
17 §
»• oo CS
•« PMR
J»
STATIC PRES OF STACK CAS
STACK PRES, ABS.
AVERAGE STACK TEMP
AV6 STACK 6AS VELOCITY
STACK AREA
STACK FLOW RATE, DRY*
ACTUAL STACK FLOW RATE
PERCENT ISOKINETIC , '
TOTAL LEAD
M6. EPA 5
TOTAL LEAD
TOTAL LEAD
EMISSION RATE
.''** FILTERABLf P«T» * :
MB. EPA 5
FILTERABLE PART.
FILTERABLE PART.
! EMISSION RATE'' 	 '''"' " •'
•.82
28,54
87.
IN-H20
IN-H6
F
68.2 FP3
1142t_ 80-IN,
1754421.
19471*8.
103.1
2.2
.0004
.096
,:? ?.•
.0012
,309

SCFH
ACFH

CR/DSCF*
LB/HR

6R/DSCF*
LB/HR

- "20.83 MM-H20 - - - : -- ^-- -• ; : ^
724,91 MM-HG _;
31. C
20.8 -HP8 „
,737 SO-M -j
49680. 3CMH 'r
55138, ACMH ' ' ' ' "
•
103.1 '
2.2 ;
4
->?$.'<*•• K-W^i,-' 1-- .. _•£ . - W . ,
.880 HG/03C^
, 3
.04 KG/HR 1 5
o
j

2.826 CG/DSCM
.14 KG/HR | 1
	 " ' *"• ' • •-," • " ' ' • - "'-I' •'• .-• •••,- -f- • .' r ,--rr -• - -- '|^ f<
'* ! >'
   *  68 DEC F.   29.92 IN.HG.

-------
      EXAMPLE  PARTICULATE CALCULATIONS TEST NO.  B3L-1


           BA6HOUSE NOtS OUTLET"
VOLUME OF DRV  6AS SAMPLED AT STANDARD CONDITIONS
VMSTO • (17.647  «  VM « Y * (PB + PM / 13.6))  /  (TM  4>  460.)


                   	65..J)tft-*-JL«.tl.e .*... t Jt9^60  ».6.414 _/ 13 . 61
                   •«««•••••»••««••>•••»••«•»»»•««*»-••»•»*••••• >

                          (  74. » 460.)
VMSTO *
                                                                              03CF
WQLUMt Qf MATER  VAPOR AT iTftkflAJtO CONDITIONS


Vt»C • .04707  * VLC
PERCENT MOISTURE IN STACK CAS

> 87.485 * 1.8S
1
MQLE FRACTION OF DRY STACK SAS
FMO • (100. - BMO) / 100.
" " "• ' tOO.» 2,1 '. ••*;"•? "--•"• "- • •' • ' ! •""•:;« :.-../.r.
100.

AVERAGE MOLECULAR MElCfct OF 0«f itHCH 0*i '* ' ' " ' > v ' ; * ! ' ' r
MD • (PC02 * .44) * (P02 « .32) * (PN2 * FCO) * .28
MD » ( .00*44/100) » (20*9*32/100) • ((79.1* .0) « 28/100 • 28.84
MOLECULAR HEIGHT OF STACK 6A3
MMS • MD * (1. - (BMO/100)) * 18. * (BMO/100)

99
»*
4 *
««
*«
47
«•
at
.5 '
• 4
»*
»«
11 0
f
• X
• 1
«M
1 ,
	 	 	 	 .jj
^
	 Jll
MMS «   28.84* (1. •( 2.07/100)) t  18.  •  (  2.07/100) •   20.»I

-------
     STACK GAS VELOCITY AT STACK  CONDITIONS
     0ELP * SUM* OP THE WlTfVM  *  (T8  #  tOO.JT         ;^  ,  » -   . .  ;   >
                             •            -.             : '   •*  V
  	jfj| ».JISjLf^JLjCf^lLPtJLJLL'^                      	.	
     VS * 65.49 *  .61 *  422.322  /  (SORTC  26.61  *  28.54)  *  15. •   66.23  FP3
          ._fi*JL VO.UINJIB i c_fj.o»L AT_3JACH_ JQND in ONS
     OS • VS • AS » 3600/144
    "IT*   68.137* "114?; 1609/144 #"  I¥«ft'fi.
     9TACK 6A3 VOLUMETRIC FLON  AT  STANDARD  CONDITIONS
•88TD iFTf.6«f *
         _17t647_»
     OSSTD
                       	1947178. « ^28,54
                       »••»••••«•••*••••»«•«••••••
                       (  87. » 460.)
                                                  / :ct» *
                                                  » ^ f 2,Q7/|OQ j J_
                                                                   1754421.  SCFH
CO
00
     PERCENT I80KINETIC
     ISO « (30S.56*(TS«460.))*((0.002669*VLC)«(VM*r*(PB«(PM/13.6))/(TH4460.)))/(TT*VS*PS*DN*ON)
     ISO *
                                     66. *  	66»23 •
                                                                    »  ,250 •   .250
                                                                                                             103.09 PERCENT
     PARTICULATE LOADIN6 ••""JEP* METM06 "5  UT  STANDARD CONDITIONS)
	CS_«.0,OOl_j»..MN • 15_,43_/_VMSTJ
    C8 « 0.001 *     2.2 * 15.43 /
                                                                                                                                          4S
                                        87.465 •
                                                .000 8R/DSCF
     PARTICULATE LBS/HR — EPA METHOD  5
     PMR • C3 * 033TD / (15.43  •  453.6)
    _____     70*0 »   j7S44fl^ /
                                                                                                                                           "i*
                                                                                                                                    		'5
                                                                                                                                          ~"T
                                                                                                                                          !']
                                                                                                                                          i
                                                                                                                                          i *

-------
FIELD  DATA
SAMPLING LOCATION "'"**
~ 	 * 	 ~ 	 " 	 ~ SAMPLE TYPE 	
OPERATOR
AMBIENT TEMP. (DEC, F)
: ""•-' •" ••" • DAff.rx€da. iiif.nv} ' '
STATIC PRESS. (IN. M10)
FILTER NUMBER(S)
^ STACK INSIDE DIM. (INI
PITOT TUBE COEFF.
THERM. NO.
BAGHOUSE
NOUS OUTLET
"Sf '•""-•,
LEAD
DAN FITZGERALD
70.
-.;•':• '«o.^i
-.82
•0002137
38.13
.61
174
'< • BATE' - /
RUN NUflER
PROBE LENG1
NOZZLE 4-l(
ASSUMED M01
•H « TTP1
121 1.0.
STURE
"" ' * ' 9 AnPLc OUH nUP*0CIV
PETER BOX NUMBER
PETER HEAD DIFF.
' • ' V9f IV?
B3L-2
". 5 FOOT
.250
1.5
in
FB3
1.94
• 1 '.. •• -3?V '^
"GLASS

PROBE HEATER SETTING 250.
HEATER BOX SETTING 250.
METER CALIB. FACTO* - t.OlB
READ • RECORD DATA tVtRT 7.0 MINUTES
TRAVERSE SAMPLE CLOCK GAS METER VELOCITY
POINT TIME TIME READING HEAD
CLOCK)
INIT 0 748
]&.^''.a"!ww<9*n"yt •Ki"ff9-''i->f- iswjfupi
; B-02 14.0 B02 Si
8-03 21.0 809
•> b-g4 «.v oi»
1 B-05 35.0 823
«J B-06 42.0 830
i •', z • "•?•"*•• S*tf F 'bibijj T »^»v -wH»-t3F jMBJVJI
B-06 ^ 56.0 * 844
8-09* 63.0 851
B-10 70. 0 898
B-ll 77.0 905
B-12 64.0 912
B-14 98.0 926
A-01 105.0 941
A-02 '" 112.0 948 	
A-03 119.0 1011
A-04 126.0 1018
A-06 140^0 1032
A-07 147,0 1039
	 "'A-08 154.0 1046 	 "'"**
A-09 161.0 1053
A-10 116.0 1100
•, f?. • A-il 173,* ll*I,.;'Vppf
A-12 182.0 1114 X*
A-13 189.0 1121
A-14 " 	 196,0 1128"
TOTALS 196.0
	 AVERAGE 	 ' •' ' " 	 ""
ORIFICE PRESSURE
DIFFERENTIAL
STACK
TEPP
K FACTOR
DRV GAS METER
TEMP

PUMP
VACUUM
2443.7

SAMPLE IMPINGER
BOX TEMP TEMP
•fvutmr- un.n«v* lin.ncuj WEV.rj IVEV.PJ un.pvr lucv.rj tvev.rj

567.633
^^'•i03WV ^
585.280
595*065
604.865 '"
614.600
625.050
^' m 3 99 ^1 ? ™ •••-IV"
649.939
656.000
'665.660 ••"
679.155
664.290
702.066
710.300
718.000
726.400
735.165
753.550
762.950
"773.100
763.465
793.855
^ WV^f 1' ||3
814.245
624.110
833;68J
265.650



' l«i»»V
1.250
1.600
"T761FO
1.650
1.750
' fc.'pifA^
1.650
1.650
• r."5oo~
1.500
1.350
" 1.300
1.250
,980
•"1.050"
1.150
1.250
1.930
1.400
1.450
-r.7oo~
1.800
1.800
t • f 3v
1.700
1.600
1.500
> -- -
DESIRED

5,62
7.20
7,20
7^66
8,30
-• 7,38
!70
.03
T .*t
.58
.36
Il4
.57
tilt
.24
__ '**
loi
.01
7.79
7.58
7.14
" "6.70
•B,B7
ACTUAL

5.62
7.20
7.20
7.41
7.86
•"1^7 •••OF "
8.30
7.36
-- (,,71
6,70
6.03
:T •"*' 5*81
5.58
4.36
4.69
5.14
5.57
6.24
6.46
7 .56
8.01
8.01
7.56
7.14
"" 6.70~
1 " — B.B7'


83.
63.
63.
84.
64.
09. •
65.
66.
86.
87.
67.
; 67.
67.
87.
87.
87.
66.
66 •
68.
66.
88.
69.
69.
68.
68.
87.
1 " BB»
INLET OUTLET

70. 61.
75. 63.
77. ' b5.
79. 67.
61. 69.
82. 71.
84. 73.
84. 74.
85. 74.
86. 75.
• - **• 19 »
67. 76.
85. 77.
86. T8.
87. 76.
84. 76.
66. 76.
87. 78.
87. 78.
68. 76.
68. 60.
66 • , 6v •
88. 81.
69. 61.
" 92. 61.
1 "84; " 74.


9.0
6.3
6.5
6.5
7.0
i- trf#l
t.5
7.0
6.0
6.0
5.5
5.0
4.0
~4.~5
3.0
3.0
3.5
6.0
7.0
7.0
7.0
6.5
6.0


239.
250.
250.
263.
265.
235.
283.
250.
230.
230.
C3V* -
250.
273.
280.
260.
260.
260.
260.
26o!
230.
230,
273.
260.




48.
63.
38.
36.
56.
92.
94.
9*.
92.
92.
'54, •- -^- T
96.
62.
93.
94.
36.
• 46* •' , "V
30.
90.
92.
92.
93.
94. •- • ••?•' -p
96.
96.
BO.















'»

-------
           PARTICULATE FIELD DATA • RESULTS TABULATION



PLANT- NAME AND ADDRESS               TEST TEAM LEADER
/i » "•'-
, PRESTOLITEr MANCHESTER* IONA
I TEST
B3L-2 BAGHOUSE N0*3 OUTLET
OAN FITZGERALD

••f.

. ENGLISH UNITS METRIC UNITS
ID TEST
ii TB
u1" ir
',', TT
IT NP
" ON
» CP
I ' VM
o
" VM3TO
VLC
VNC
BNO
FMD
PCC2
P02
PCO
MO
MMS
UAit
TIME-START
NET TIME OF TEST* MIN.
NET SAMPLING POINTS
SAMPLING NOZZLE DIAMETER
PITOT TUBE COEFFICIENT
DROP
	 '" VOLUME OF DRY GAS SAMPLED
AT METER CONDITIONS
VOLUME OF DRY CAS SAMPLED
AT STANDARD CONDITIONS*
TOTAL H20 COLLECTED IN
VOLUME OF MATER VAPOR
AT STANDARD CONDITIONS*
PERCENT MOISTURE BY VOLUME
MOLE FRACTION DRY CAS
PERCENT C02 BY VOL.* DRV
PERCENT 02 BY VOL** DRV
PERCENT CO BY VOL.* DRY
PERCENT N2 BY VOL.* DRV
MOLECULAR MT-DRV STACK CAS
MOLECULAR NT-STACK CAS
UO/1U/O1 Ub/lU/Ol
748 746
1140 "• . ico
196.0 196.0
28 28
1
.250 IN 6.4
.61 .81
'***' """*" ' Wr**
265*850 CU'FT 7*528
•Bjf F T™ ••«!
238.957 SCF 7.333
54.1 54.1
f :
2.546 SCF .072
.97 .97
.990 .990
.00 .00
20.90 20.90
.00 .00
79.10 •"" "79.10
28.64 28.64
28.73 28.73

i
MM
"*"^
MM'MCU '•;•• < " f- .- " * '*?y ' " <;?••'* B- '« * : '. • -' '• ' ««V',!f.'
CU-M
•CM

^ ... .--... - >• r v -S-." •
SCM ;;
»




' v

-------

$•'$•'• '


'•' !
9
A
T
1
t ?* ' "
O
1
2
1
4
* ^ • ".'
8
7 -
ft ^J
2
ii
4
7
1
t
0
2
9
4
5
4
7
PB
PSI
PS
ts
vs
AS
"xrssTtr
08
ISO
HN ""
C0 ••••'f^-
PMR
MN
C8
PMR
-y





BAROMETRIC PRESSURE
STATIC PRES OF STACK
STACK PRES. ABS.
28.73 IN-HG
GAS ».82 IN-H20
28.67 IN-H6
"" AVERAGE STACK TEMP " 6b. F
AV6 STACK OAS VELOCITY 68.7 FPS
STACK AREA
1142. SO-IN
STACK FLOW MATCf OKV* ir?b700. SCFM
ACTUAL STACK FLOW RATE 1959588. ACFH
PERCENT I80Kt«tlC\n
TOTAL LtAD '""*""
M6. EPA S
. • T" f*TIIB'vK*l'lt<*-"' yf*H«W|P
TOTAL LEAD
EMISSION NAtE
FILTERABLE PART.
"••"**? BB»' IfH •« • " >vAv'OMPP'
.049 LB/HR
13.1
,;3r-T| >-^>-lllPV 'Vf ••' ' '
•;;; .0006 8R/DSCF*
.200 LB/HR
^•T»T" '""^

"""'

'.S1 --"••''

729.74 MM-H6
»
•20.83 HM-H20 '
••'-•• 7-7 -'•••• ---;• " 	 -'"n »N
728.21 KM-HC
30. C
20.9 NFS
.737 80»M '
*
50§77. SCWH " " " "n
t «
SS490. ACMH II
-v# ." f 7- • 7
lot** . ;
. „ '- •.:«' "
I*
f4
.02 K6/NR 1
to
is.i ;;
1.787 M6/D8CP . ;
3 T
.09 K6/HR >•
V*
40
. . ,f, << ^ .~ . r IT ^ .-vr •• -^'r^ ' • - 4.
4t
4 *
44
47
41
SO
92
P4
9*
* .«
B*
• O
• 1
64
O '..-•;• s?
1 ' • *
H2
SI
54
31






• 9
M
72
74
71

-------
EXAMPLE PARTICIPATE CALCULATIONS TEST NO. B3L-2



     BA6HOUSE N0*3 OUTLET
X" " "•" ; / .''. • ' ""*"" ! : ' " "
" 	 VOLUME OF DRf GAS SAMPLED
VMSTO • (17.647 • VM * V
17.647 * 265.

1
1
1
I VOLUME OF MATER VAPOR AT
i
i VNC • . U«/0/ * VLt
! VNC « .04707 * 54. •
If V "'f^'- ':--* ' ' "1"^"''\ - ; *~ • •' ™*V " -rt-'"
10
21
	 ; ;• •;,. ,. • ' • •• " • '; = v:; • 	 r 	 	 : "? ^
AT STANDARD CONDITIONS " "~ 	 ~"~
* (PB * PM / 13.6)) / (TM 4 460.)
850 * 1.018 • ( 28.73 * 6,672 / 13.6)

( 79. * 460.)
STANDARD CONDITIONS
2.55 SCF
W&*"f *' •«•• . '"?f "" 	 •''"•.'• •'• " " •'.-'•' " • : :'•'•'• ""I- •• "'"' ••"".•• • V' " •!.---
„' " PERCENT MOISTURE IN STACK bA9
" BNO • (100. * VMC) / (VMSTD t VKC)
! 100, ft l,n

„ • ' 1 " 259.957 » 2.
UD
» |\J
30
• D9 0VBr^lUT

55
»
MOLE FRACTION OF ORT STACK GAS
,. FHD * doo. • BMOI / 100.
!! 100. - i.o
FJ? 	 « . " mu •, -•••^•••^••••••••••MI
100.
39
AD
',[ AVERAGE MOLECULAR WEIGHT
MO • (PC02 * .44) * (P02
48
7
•
I MOLECULAR HEIGHT OF STACK
~ — ~~ — HITS TT mo r~rrr~^ TBWO/TOW
" "MNS * 28.84* (1. -( .97
«5 . - .„.
ft
...
•JW* -• 9'990 ^--- •"' -.. — .- ••-.- -- 	 --?-•'• •• - - --• 	 ••-,.- 7_J!" v. .. . - - 	 r|o
.
OF DRV STACK GAS
* .38) * (PN2 * PCO) • .21' *

' -, • .
6AS
)) * 18, • (BHO/100) ' "i;
/100)) * 18. • ( .97/100) • 28.73 \','t
• '•'.'• °?

-------
STACK 6AS VELOCITY AT STACK CONDITIONS



OELP * SUM. OP THE 80RT(VH * (TS » 460.))
. . 1, . , . ....... .,..
, VS * 85.49 * CP * DELP / (
;
i STACK 6AS VOLUMETRIC FLO*
rr OS » VS' • *8 • 3600/144
',', 08 • 68.66 * 1142. 3600

,, 08STD • 17.647 * OS • PS «
"*.T • • <•• , , . . • ,^JB v. • -™
i7,»4f • ; 1939

I B6.
PERCENT ISOKINETIC
1 * *
" S (305. 58* ( 86. +460.

PARTICULATE LOADING •- EPA
CS • 0.001 • MN * 15*41 /
CS * 0.001 • 3.2 • 15.
" PARTICIPATE LBS/HR •* EPA
PMR * CS * OSSTD / t!3!43
". PMR • .900 • 179679
" * . "^ "*
it

SORfCMNS * PS) * PNT8)

AT STACK CONDITIONS
/144 « 1959588. ACPH
- '^Vf '•* • . .'*'*'" " ' • ' ' • * •• " • x, ••
'"!•'•
(1. » (BMO/100)) / (TS * 460.)
*v!'--*r*?*'"r|fw-':''*:;" ...-,*$«;• ,?•»•; .>•" , •JT. ' y^ ^ = •? 5-^ - >^^ V.'- *-• " Tvnv7-.v- ' *, ' •
588. * 28.67 « (1. - ( .97/100))

* *bO.)
^?»*^v«^'- ,^f ','i^^t ' ' ijr^ff. * • ,T" ,- "• . "^ ^ ' ,f ' • - ... v: ij"v . -. ,--•.?. T* v " ***• 7^
))*((0. 002669* 54.)*{ 265. 850*1. 018*( 28.73«( 6.672/13.6)) /( 79. +460*)))
196. 4 68.66 * 28.67 • .230 * .230
METHOD 3 (AT STANDARD CONDITIONS)
VMSTB
43 / 238. 957 '• .000 GR/DSCF
METHOD 3
» 433.6) 	
9. / (13.43 * 453.6) * .05
1


f\

0
z
-I
4
•
•
7
1 •
*t
zo
21
zz
21
24
29
7«
2
2
i
1
:
7
•
t
0
4 I
::
»s
44
47
*
fj
'
2
1
«
«B
•
•
9
o
t
• i
<4
«•
7
i
»
70
71
'I
r •
^n
"»

-------
FIELD  DATA
^T — ! 	 ' — : 	 PCTOTI 	 ~ PRESTOLITE, MANCKEmnmOITA 	 	 OAT1 	 " 99/19/91 	 • ' '* ,\
SAMPLING LOCATION BAGHOUSE *3 OUTLET RUN NUMBER B3L-3
SAMPLE TYPE LEAD ~ 	 PROBE LENGTH S TYPE 5 FOOT GLASS
OPERATOR DAN FITZGERALD NOZZLE 4-1021 1.0. .250
AMBIENT TEMP. (DEC. F) 80. ASSUMED MOISTURE 1.5
	 ' 	 ' 	 BAH. PRESS. (IN. H6) 	 	 28.83 	 	 	 	 SAMPLE BOX RUBBER" 	 - ... , 	
STATIC PRESS. (IN. M20) -.82 METER BOX NUMBER F83
FILTER NUMBER(S) D0001993 METER HEAD DIFF. 1.94
STACK INSIDE DIM. (IN) " 38.13 "."Ofl "' ""
PITOT TUBE COEFF. .81 PROBE HEATER SETTING 250.
, THERM. NO. 174 HEATER BOX SETTING 250.
I METER CALIB* FACTOR 1.018 K FACTOR 2443.7
READ 8 RECORD DATA EVERY 3.5 MINUTES
. 	 " " ' •"' ' 	 ""•" ' ""' " ' ' "
TRAVERSE SAMPLE CLOCK GAS METER VELOCITY ORIFICE PRESSURE STACK DRV CAS METER PUMP SAMPLE IMPINGER
. POINT TIME TIME READING HEAD DIFFERENTIAL TEMP TEMP VACUUM BOX TEMP TEMP
, T '"••' "!' NU. "'. •~>l. (WIN.'l' (2»»NR " '"'•! (CU.PT;/ "'tlWrfWWI) "'" (IN.H10) 	 (UC6.P7 C&**.P> IWIfl
DESIRED ACTUAL INLET OUTLET
i«f'«ira«*ri lucw.rj -
1 INIT 0 1300 833.980
j '". 	 " A*01 "-s" " 5.5 !*"' 13U5"-"'T 	 "" 840*4*3 '4 ""•'„: '14 l^O "*"' ' 4,?f ' 4,91"' 88. •(•' 	 • •!• ^" " A-03 15.5 1316 854.100 1.300 5.79 5.79 89. 86. 80.
1 • A-04 '"' 22.0 	 1322 861.225 1.350 6.01 "6.01 89. 90. " 81;
2 ^ A-05 27.5 1327 868.350 1.350 6.01 6.01 89. 91. 81.
A-06 33.0 1333 875.605 1.400 6.22 6.22 90. 93. 81.
," '•"""•""""'' A»07 '",l"» '"38. 3"'!!*M338 ".r1*— 883. 860 ' 1.550 " '8,89 ' 	 " 8.89 90, ''94. ' ••".'."".Bl •• '"?' -"»
A-08 44.0 1344 891.130 1.700 7.55 7.55 90. 96. 81.
A-09 49.5 1349 899.400 1.800 8.00 8.00 90. 97. 81.
, A-10 55.0 1355 907.380 1.750 7.76 7.76 91. 97. " 82.
A-ll 60.5 1400 915.345 1.700 7.54 7.54 91. 98. 82.
A-12 66.0 1406 923.110 1.600 7.10 7.10 91. 98. 83.
,"" ' ' AM3 """""71,5 	 1411 '' ""i '930.545 .. ' 1,430 	 .43'" ' 6.43 "91. 	 98." ' 84; '"" — ' 1
A-14 77.0 1417 937.949 1.450 .43 6.43 91. 98. 84.
B-01 82.5 1439 . 944.580 1.200 .33 5.33 90. 94. 84.
„ 	 B-02 88.0" "1445 951.615 1.300 .79 5.79 89. ~ 90; " 84.
8-03 93.5 1450 958.890 1.400 .22 6.22 90. 91. 84.
„ B-04 99.0 1456 966.540 1.550 .89 6.89 90. 95. 84.
4i • 6*wi - iu^.5 rt34i . 97»»4+« ~i.7vw 7.55 7.55 90. 97. 64.
B-06 110.0 1507 982.610 1.750 7.79 7.79 89. 98. 84.
8-07 115.5 1512 990.870 1.800 8.01 8.01 89. 98. 84.
* ' "" B-08 	 121.0 '1518 ' '"998.970 1.750 7.79 7.79 89. 98. 84.
B-09 126.5 1523 6.855 1.650 7.34 7.34 89. 98. 84.
B-10 132.0 1529 14.660 1.550 6.90 6.90 89. 98. 84.
" B-12 143.0 1540 29.230 1.400 6.22 6.22 90. 100. 86.
B-13 146.5 1545 35.680 1.300 5.79 5.79 89. 100. 86.
^•v 
-------
           PARTICIPATE FIELD DATA I RESULTS TABULATION



PLANT* NAME AND ADDRESS               TEST TEAM LEADER
1 PRESTOLITE. MANCHESTER* IONA
TEST

B3L-3 BAGHOU8E *3 OUTLET

i TEST DATE
TB
"•"• ' TF ~.L
I TT
7 NP
. •- : *- '. i " '-•'!
o
i ON
I
CP
27
11 vM
3  PC02
! P02
*I PCO
St
, PN2
!1 MO
i« MN3
TIME-START
NET TIME OF TIBt, MIN* '•§£
NET SAMPLING POINTS
SAMPLING NOZZLE DIAMETER
PITOT TUBE COEFFICIENT
DROP
VuLunt Of DKT 6*8 SAMPLED
AT METER CONDITIONS
VOLUME OF DRV 6*8 SAMPLED
AT STANDARD cOnOITiOwS*
TOTAL H20 COLLECTED IN
VOLUME OF NATER VAPOR
" AT STANDARD CONDITIONS*
PERCENT MOISTURE BY VOLUME
MOLE FRACTION DftV GAS
PERCENT C02 BT VOL.* DRV
PERCENT 02 BY VOL.t DRY
PERCENT CO BY VOL.. DRY
PERCENT N2 BY VOL.. DRY
MOLECULAR NT-DRY STACK GA8
MOLECULAR NT-STACK GAS
DAN FITZGERALD

ENGLISH UNITS
06/10/01
1300
irv.i; 1531 • ' *
154.0
28
.250 IN
.81
^. -.,., ,^«

200.654 SCF
44.3
;«
2.085 SCF
1.03
.990
• 	 .00 	 "
20.90
.00
79.10
28.84
28.72
. j

METRIC UNITS
06/1 0/il
1300
- ..., 1331 7 f • •'.-!*.-•. ,
154.0
28
6.4 MM
.81
""' ' ""' T1I.O *JW*HIU '•'' " " "'"' " *••'" •" '*-' ' "• '#""' 	 	 	 ' 	 "!;'""w
5.923 CU*H
5.682 8CM
44.3
.059 8CM
1.03
.990
20.90
.00
28.84
28.72










1



-------
PB        BAROMETRIC PRESSURE


PSI       STATIC PRES OF STACK 6AS
                                 28.83  IN-H6


                                  -.82  IN-H20
                                                                732.28   MM-H6


                                                                •20.83   MM-H20
PS
is


VS
STACK PRES, ABS.
                                           28.T7  IN-H8
                        TEMP
AVC STACK GAS VELOCITY
                                           68.7   FP8
                                                     730.75  MM-H6

                                                       jjr;c

                                                       20.9   HP3
AS
U39TD


OS
 STACK AREA


"STACK PLUW fcflttr


 ACTUAL STACK FLOW RATE
                               1142.   SQ-IM


                            T792B8T;	
                                                         .737 80-M
                            1961047,
ACFH
                                                             SH7b"».


                                                             5S531.
                                                                        StMrt"
                                                              ACMH
ISO
MN
PERCENT fSOKINCTlC
                                           101.•
                                                      101.4
          TUTAL LtAU
            M6. EPA S
          TOTAL LEAD
                                                                  5.3
  EMISSION RATE

FILTERABLE PART.
                                   .105   LB/HR
                                                                    .09   K6/HR
                                 11.3
                                 111 r111
                                                                 11.3
          FILTERABLE PART.
PMR       FILTERABLE PART.
            EMISSION RATE
   •  68 OE6 F,  I«.ti
                                   .0009 6R/OSCF*
                                                                  1.989  H6/D8CM
                                              ,223   LB/HR
                                                         .10  K6/NR
                                                                                                        ty '

-------
            EXAMPLE ^ARTICULATE CALCULATIONS  TEST  NO.  B3L-3


                 BA6NOUSE i3 OUTLET
     """VOLTliflE OF" D^T SA^ JJAM^Lto  XT  STfcNnAhU


      VMSTD * (17.647 * VN • Y *  (FB  *  PM  /  13.*))  /  (TM * 460.)
      VMSTO *
                17.647 I   tt^.UO  *  1.018  •  (  20,63 * 6.613 /
                                                               *    200.65*  D8CF
      .

VOLUHE OF HATER VA
                                         CONDITION*
VHC * .04797 * VLC


VNC • .04707 •   44.  •
                               2.0» ttf
      PEHCENT MOISTURE IN 8TACK  B*»


      8NO • (100. * VNC) /  (VMSTD *  VNC}
I
vo
-0
                100, *
          •..«.»»*....«**.»».4»»«»«»»** ••  1,03 MRCENT
      MOLE FRACTION OP DRY
            (100. • fcnO) /  1001


                100. »   1.0
                    I

                     100.
      AVERA6E MOLECULAR HEIGHT  OF  DRY  STACK  6AS
      MO • (PC02 • ,44) *  CF02  *  .32)  *  (FN2 * FCO) • .88


      MO » t  ;00«44/100")  * t20i*l32/100)  * C(79;i« .01
        "'    • • '       .   "i!".^ n i  "";'  •!..«  «• ") i

      MOLECULAR HCICHT OF STACK 6AS
                                    'It.
      MN8 •  2B.S4*  (i. -(  1.03/100))  * IB. • ( 1.03/100) •   28.TZ

-------
          STACK GAS VELOCITY AT STACK  CONDITIONS

          OELP « SUM. OP THE SORT(VH * (TS  *  460.))
          VS * 85.49 « CP * DELP /  (SORT(MNS  *  PS)  *  PNTS)              '

          VS » 05.** *                               l  in
i*«
          PERCENT ISOKINETIC
      ^o
      00         (30S.58*(  90.+460.))*((0.002669*    4«.)*(   209.160*1.018*(  28.63«(   6.613/13.6))/(  09.4460.)))
     	 18V mmmmmmwmmmmmmmmmmmmmmmmmmm	wmmmmu»»*»*m**m»»m*»***m*»»mmwr..m*.mmmm*mmmmmm»mmmm**mmmm,mmm*m. *  Hli
-------
FIELD  DATA
« SAMPLING LOCATION
' 	 " 	 SAMPLE TYPE 	 '
, OPERATOR
. AMBIENT TEMP. (DEC. F)
^~v,.: >••-{'• - • BAR.rnE9a.iiit«nvj ::
STATIC PRESS. (IN.HBO)
FILTER NUMBER (S)
STACK iNSlOfc DIM. (IN)
PITOT TUBE COEFP.
THERM. NO.
METER CALIB. FACTO* ^
READ ft RECORD DATA jf
BA6HOUSE 'N003 OUTLET
LtAO
DAN FITZGERALD
70.
-!82
00002222
30.13 .00
.81
174
t*lK!l»9 MINUTES
TRAVERSE SAMPLE CLOCK GAS METER VELOCITY
POINT TIME TIME READING HEAD
•' •' , ;.'' ' '" CLOCK) ''" ' '• • •''"
INIT 0 850
^ ' ' ''.".' B-02 '; -- lllo 901 tV'X'
B-03 16.5 906
	 •"'" ' B-04 	 " 22.0 ' 912 	 ""
,y B-05 27.5 917
1 B-06 33.0 923
^ B-OB 44.0 ' 934
B-09 49.5 939
B-10 	 '55.0 945
B-ll 60.5 950
8-12 66.0 956
B-14 77.0 1024
•01 82.5 1034
-02 88. 0 1040
-03 93.5 1045
-04 99.0 1051
-06 110.0 1102
-07 115.5 1107
	 " -08 	 121.0 1113 	 	
-09 126.5 1118
-10 132.0 1124
"• " ' ' ' Ml 13/.5 11*9 5M^
•12 143.0 1135 '5
•13 148.5 1140
• 14 ••'•' 154.0 	 1146
I'll TOTALS 154.0
„«„„„
44.909
(R«?51 »54P ~ •T-WttlOO'
58.610 1.350
66.100 1*600
	 73.800 l'."600'
81.675 1.700
89.690 1.750
'.£ ^ffjVJV • l'«B3U
106.145 1.850
114.160 1.750
121.880 ' 1V600
129.600 1.600
137.110 1.500
15U28S 1*300
157.435 1.000
164.450 1.200
171.180 1.300
178.185 1.300
vii3.l"»w . • 1..9W
192.475 1.400
199.965 1.500
208.120 1.800
216.400 1.850
224.650 1.800
f'232.765 1.8UO
240.850 1.750
248.460 1.550
256.132 1.550
211.223




B IWiiW




ORIFICE PRESSURE
DIFFERENTIAL
DESIRED

5.96
7.06
7.06
7.50
7.72
" 0.10
8.16
7.72
7.06
7.06
6.62
4 . 1 B
5.73
4.41
5.29
5.72
5.72
fcllb
6.60
7.92
7!91
'" 7.91
7.69
6.80

•0. r^
ACTUAL

5.96
7.06
7^50
7.72
*•* o • 1 0
8.16
7.72
7.06
7.06
6.62
0.10
5.73
4.41
5.29
5.72
5.72
6.16
6.60
~ 	 7.92~
8.14
7.91
	 7.91
7.69
6.80
" 	 6.80"
., • " Bit r* •





STACK
TEMP
0EB.F

89.
89.
" 89.
89.
89.
89.
89.
89^
89.
89.
89.
89.
" 89.
90.
90.
90.
90.
90.
90.
91.
91.
92.
92.

" - " 'BUTE
RUN NUMBER
PROBE LENeTH » TYPE
NOZZLE 4-1021 I.D.
ASSUMED MOISTURE
SAPPIC BUH NUMBER
METER BOX NUMBER
METER HEAD OIFF.
PROBE HEATER SETTING
HEATER BOX SETTING
K FACTOR
VBf llf
B3L-4
5 FOOT
.250
1.5
FB3
1.94
290.
250.
1421.7
BI" ' 	 	 'r"-"'^>
~cnss


* <"•
. i
DRY GAS METER PUMP SAMPLE IMPfNGER
TEMP VACUUM BOX TEMP TEMP
I IDEVtPt • • l»H*fW* I
INLET OUTLET

<& ^ -tJ'J r ?«Wi' -^ .••! '•'
76. 68. 5.
82. 69. 6.
«; TT. ^.s~
88. 72. 6.
89. 74. 6.
^i. Va* ••• f»"
92. 77. 7.
92. 78. 6.
92. 80. 6.0
92. 80. 6.0
92. 80. 5.5
93. 00. " :9.0
89. 82. 5.0
91. 82. 4.0
92. 83. 4.5
96. 84. 5.0
98. 84. 5.0
lOo! 87^ 5.0
101. 88. 5.5
102. 69. 7.0
102. 89. 7.0
102. 90. 7.0
103. 91. 6.9
104. 93. 6.0
~~ ~IU4." - • 9T; 6;o



•BBJ' ~r~'
290*
290.
25o|
270.
280.
300.
30D.
300.
300.
350.
250.
320i
340. -
350.
350.
350.
350.
350.
350.
390.
350.
350.
31*.


•65.
65.
66.
66.
65.
61.
59.
57. *
57.
58.
•96.
46.
50.
57.
56.
59.
0v • R W
61.
60.
57.
56.
56.
">96. •' •? ~i
56.
97.
57.
t
7
•19. ~- • -•-.•>
	 P

-------
           PARTICULATE FIELD DATA I RESULTS TABULATION



PLANT" NAME AND ADDRESS               TEST TEAM LEADER
PRE8TOLITE, MANCHESTER, IONA
TEST

Tt3T
TB
TF
TT
NP
ON
CP
B3L-4 BA6HOU8E N0»3 OUTLET

DATE
TIME-START
NET TIME OF TEST, MIN. '
NET SAMPLING POINTS
SAMPLING NOZZLE DIAMETER
PITOT TUBE COEFFICIENT
DROP
1
VMSTO
VLC
VNC
BMO
FMD
P02
PCO
PNZ
MO
MHS
VOLUME OF DRY GAS SAMPLED
AT METER CONDITIONS
VOLUME OF DRY GAS SAMPLED
AT STANDARD CONDITIONS*
TOTAL H20 COLLECTED IN
i«rjm*ens AMD. SILICA feELV^L
VOLUME OF NATER VAPOR
AT STANDARD CONDITIONS*
PERCENT MOISTURE BY VOLUME
MOLE FRACTION DRV CAS
PtHttwl Ci»i BT VOL*, DRV
PERCENT 02 BY VOL., DRV
PERCENT CO BY VOL., DRV
PERCENT N2 B¥ VOL., OUT
MOLECULAR NT-DRY STACK GAS
MOLECULAR NT-STACK GAS
DAN FITZGERALD

ENGLISH UNITS
Ob/11/81
850
" 1 HB
154.0
28
.290 IN
.01

211.223 CU-FT
2*4, 0*9 SCF
51. T
2.434 SCF
1.10
.90.
.00
20.90
.00
T9.ro 	
20.04
20. Tl
. ': , ' . '*

METRIC UNITS
Ob/11/01
154.0
20
6.« MM
.01
...T
5.901 CU-M


1 0
1 I
l«
i:
14

10
*^


JW.f C -. '"" " ••«<•• V • " "'I :f ' • • • » 41
5.TT9 8CM
51. T
i
.069 8CM
1.10
.900
.00 .......
20.90
	 ' j
"" ' 7TiIO"' 	 """ " - 	 	 *
20.04
20. Tl



'V

-------
PB BAROMETRIC PRESSURE
PSI STATIC PRES OF STACK
P» STACK PRES* ABS*
*
28.95 1N-M6
6A8 -.82 IN-H20
28.89 IN-HB
"" TS AVERA6F. STACK TEMP 90. F
VS AVB STACK OAS VELOCITY 69.8 FPS
AS STACK AREA
1142. 80-IN
od&Tb STACK ^LOH RAtt» btY* lazszvt. SCFH
OS ACTUAL STACK FLON RATE 1991431. ACFH
ISO PERCENT ISOKlRCtlC ^
MN fOtAL LtAD
M6. EPA 9
ss-Tr--'- C|F- "W-> T- TOTAL •tHWwr*~**f- •"• "WB1.
PMR TOTAL LEAD
EMISSION RATE
MN FILTERABLE PART.
,..^V..,. Vf,r.:^,r |^j^ ep(| .j . , ^ff^ijflJJ,
CS FILTERABLE FART.
L PMR FILTERABLE PART.
0 EMISSION RATE
* 6ft DffO F, 29.9Z IN. MS.
^ 101.3
4.i
.092 LB/HR
16.7
^ .0013 BR/DSCF*
.329 LB/HR
IPf'?^1*1" f'-T^y "-1 ••' T--r
735.33 MM*H6
•20.83 MM-H20 '
733.80 MM-MB
32 • C
21.3 FPS
.737 80-M
51*86. StMH
56391. ACMH
101. S
4.7
.04 K6/HR
16.7
2.890 P6/08CM
.15 K6/HR


(s








r^, ,^:« v^^,,): ..r-^,.,^^.,.^, _,,- -, .f_ , . ;..t ..

1 '••'-•'''.•,

i








-------
                EXAMPLE PARTICIPATE CALCULATIONS TEST NO. B3L-4

                     BAGHOUSE N0*3 OUTLET
                                    JTT 4 f ANbARD CONbll
          VOL         i

          VM3TD « (17.647 • VM * Y • (PB * *M / IS. 6)) /  (TM * 460.)
          VMSTO
                    17.647 *   211.223 • 1.018 • ( 28.95 » 6.7SS /  13.6)
                                   I00. » 46V.J
204.064 D8CF
          VOLUME OF MATER VAPO* AT STANDARD CONDITIONS
          VWC
          VNC * .04707 *   52. •   2.43 SCF
10

II
          BNO • (100. • VNC) / (VMSTO * VNC)
                    100* •'   2.43                  '
          BNO «»-*•---.-»«•—«»••••••»«>.»»«  1.18 PERCENT
                     204.06% »   £.43
     '10-
          MOLE FRACTION OP OUT STACK 8A8
          AVERAGE MOLECULAR NEI6HT OP DRT STACK GAS
          MD • (PC02 * .44) * (P02 * .32) * (PN2 * PCO) • .28

          tab • (  .00*44/100) »'' 120.9*32/100) * C(7*.l* .0) »"28/100"«   28.81
          MOLECULAR HEIGHT OP STACK GAS
                                            » (BWO/100)

          MNS *  28.84* (1. •( 1.16/100)) * 18. * C 1.18/100) «   28.71

-------
        STACK 6*3 VELOCITY  AT  STACK  CONDITIONS
        DELP • SUM. OF THE  SORTCVH * (TS * 460.))
 VS « 65.49 * CP  *  DELP / (80RT(MM8 * PS) • PNTS)
~V4 * B5.49 *   .fcli   612.546 ^~(46*itT 86.71 * 2B.B9T"

 STACK 6AS VOLUMETRIC  FLOW AT STACK CONDITIONS
"Us a VS * AS * 3600/144~~
 OS •   69.78 •   U42. 3600/144 « '   1991431. ACFH
      •(••"."   •'.-• w:';W  •• •iifjy.?"  ' *,-«?•> :  J4"sr*": >    _•        ••-,•-,-,-.•

 StACK cAa vtJuuntlKiC
 Q8STO •17.647 •08 * PS •(i.-* (•NO/100)) /(T8»  460.)
           17.647 *    I9914SI. *  10.89 * (t. •  (1*18/100))
^asa^O •••••••••»*••**;•••*•••••**•••••*-•••*•••••--•--•••- «	1S252«9_. |_CF_M	
                     (%ti. * 46o.j

 PERCENT ISOK1NETIC

	(305,56*(  90.»460.))*((0.002669*   52.)*(   211.223*1,01B*( 28.95»(   6.788/13	
                                     154. *     69.78  •    28.89 «  .250 •  .250

 PARTICULATE  LOADIN6 «- EPA METHOD 5 (AT STANDARD CONDITIONS)	
 CS • 0.001 * MN  •  15.43 / VMSTD
~tS~ * O.OOl *     4.7  * 1S.*!S /   H04.0%9 *      .000  6R/03Cf    "                                         ""      ' ~"     ""

 PARTICULATE  LBS/HR »• EPA METHOD 5
 PIW* C3~~" 043TO T (15.43 * 453.6)            ~"                        .----                           __._	_  .                -
 PMR •     .000 •    1625249. / (19.43 • 453.6)  •	.09	




                                                                                                                                        ',•*'
O
U)

-------
FIELD  DATA
r • •• ' PLAItl ^KCalULilCr WUhCHlSICWf IUHN ' II* 1C • VVIIfVl :  "02 11.0 1310 269.745
, ' -03 16.5 1313 276.670
," 0 -04 22.0 1321 283.615
^. -05 27.3 1336 290.800
,. -06 33.0 1332 298.230
,, T • »uJ ao.i liif ..="•>> '• -303. 963
, -08 44.0 1343 314.293
-09 49.5 1348 322.603
, -10 55.0 1354 330.940
, -11 60.5 1339 339.020
•12 66.0 1405 346.933
3 ' "13 Ji.4 " I4l!> ' "• • 334.603
-14 77.0 1416 362.295
, B-01 82.5 1446 368.955
, B-02 88.0 '1452 376.445
4 B-03 93.3 1457 384.260
B-04 99.0 1503 392.380
• T B-ua io«.3 - - livi • "' ^wu»3j« '
B-06 110.0 1514 408.710
B-04 115.3 1519 416.960
. B-OB 121.0 1523 	 425.160
. B-09 126^5 1530 433.050
. 6-10 132.0 1536 440.480
, B«n iat.4 i4*4 ••• »»7.745
B-12 143.0 1347 455.035
8-13 140.5 1552 461.947
I.IOD 4.56 4«0* ^J. ^»» ^4tf 'J.W CV3i ' »3. ,-,,.,,
.200 . 5.30 .30 93. 96. 93. 3.5 280. 65.
.250 5.32 .52 93. 99. 93. 3.3 260. 63. !;;
r.250 ^.51 ~5.Sr ~94. 102." 93. ^-3.1 230; 83. ' 	 "
.350 5.96 .96 94. 104. 93. 3.5 260. 65.
.450 6.40 .40 94. 104. 94. 4.0 280. 65.
.600 7.0* .04 •M. id4. ' '" 4;*. " r
.850 8.14 .14 95. 106. 94.
.850 8.14 .14 95. 106. 94.
r.BSO 8.I4-" 8.14 "93. I~06. 96.
.750 7.69 7.69 96. 106. 96.
.650 7.25 7.25 96. 108. 97.
.330 a.o4 b.oe "»i. iu8. 97.
.550 6.82 6.82 96. 107. 97.
.200 5.28 5.28 95. 104. 97.
.500 6.59 6.59 . 96. 98. 96.
.650 7.26 7.26 93. 99. 96.
.700 . 7.48 7.48 93. 101. 96.
,*uw ' J.^l •*" T.^I * "»•• tOC. *6.
.800 7.91 7.91 96. 103. 96.
.830 8.13 8.13 93. 104. 96.
.800 7.92 7.92 93. 103. 96.
.600 7.04 7.04 93. 104. 96.
.300 6.59 6.59 96. 105. 96.
.4vv o.ie o.ie ^3. iu3. +b»
.400 6.16 6.16 95. 105. 96.
.250 5.30 5.50 93. 103. 96.
• •^ COW. O3. ' •
.0 280. 63.
.0 280. 63.
,TT 280. 65.
.3 280. 65.
.5 270. 66.
«v 
-------
           PARTICULATE FIELD DATA 8 RESULTS TABULATION



PLANT- NAME AND ADDRESS               TEST TEAM LEADER
f " PRESTOLITE* MANCHESTER *'*lt)NA^ ' ^**
TEST

TEST
TB
? " TF~
TT
NP
*. ' » £
ON
CP
.
1 VM
I-1
o
VMSTD
VLC
VNC
BNO
FMO
PC02
P02
PCO
MD
MM 8
B3P-1 BACHOUSE NO* 3 OUTLET
f • • ~ <-Tf-.;l .if^SlffJ^!*:: ~m*&f-~ ' 'fT^k™--: ~f--
WTE " 	 " 	 ' 	 - 	 ;' '
TIME-START
NET TIME OF Ttlf» KlN» |1
NET SAMPLING POINTS
SAMPLING NOZZLE DIAMETER
PITOT TUBE COEFFICIENT
DROP
VOLUME iif Out 6AS SAWPLfcO
AT METER CONDITIONS
VOLUME OF DRY CAS SAMPLED
AT STANDARD CONDITIONS*
TOTAL H20 COLLECTED IN
VOLUME OF NATER VAPOR
AT STANDARD CONDITIONS* ""
PERCENT MOISTURE BY VOLUME
MOLE FRACTION DRY CAS
PERCENT C02 BT VOL.? DRY
PERCENT 02 BY VOL.» DRV
PERCENT CO BY VOL.* DRY
PERCENT N2 BY VOL.* DRY
MOLECULAR NT-DRY STACK CAS
MOLECULAR NT-STACK CAS
DAN FITZGERALD

ENGLISH UNITS
Db/ 11/81
1239
148.3
27
•230 IN
.81
*
jf05.43J CU— Ft
194.318 SCF
43.3
2.048 SCF
1.04
fST'7'--'* : '
.00
20.90
.00
	 7^.10 •""
28.84
28.72
t\j _t Kj.'-" . "i'-

METRIC UNITS
	 06/Il/fll
1259
-- 1591 ' T ' ' _
148.3
27
*.4 MM 4
.81

3.818 CU-N
3.302 8CM
43.3 J
.038 8CM
1.04
' • - T - . . r i • % i ^"'7
.990
.00
20.90
.00
79.10
28.84
28.72


0
2
j
t
0
• 2
11
t<*
f 7
21
2*
JO
11
31
14
4
37
»•
• t
• 0
• 7
1
:i
JT
0
2
• 4
ft
**
It
• 0
• 2
• S
• 4
c$
7
TO
n
71
74
7?
7*

-------
PB BAROMETRIC PRESSURE
P8I STATIC PRE8 OF STACK GAS
PS STACK PRE8, ABS.
13 AVERAGE STACK TEMP
VS AVG STACK GAS VELOCITY
AS STACK AREA
B3STD StAtk FLON ft«TE» UKY»
OS ACTUAL STACK FLON RATE
ISO PERCENT ISOKINETtC.
MN f1 IL * t^ABUt KAKi
MG. EPA 5
'••- C9 • • ' riUIKKMBLK 'FPIli -firer*ir:--«-r"^v*
PMR FILTERABLE PART
MN CONO. INORGANIC
fr C* CONO. INORGANIC '
1 ... .
£ PMR CONO. INORGANIC
S EMISSION RATE
MN COND. ORGANIC
MG. EPA 5
C8 CONO. ORGANIC
... ppu , . - ,,.> CONU. OHVMNlt" "•""." T" '" "!"W ,
EMISSION RATE
MN TOtAL PAKllCutAlt
MG. EPA 5
PMR TOTAL PARTICULAR
	 EMISSION RATE 	 "
* 68 OE6 Ff 29.92 IN.HG.
' ... - ;.; *''•' '


88.95 IN-HG 735.33
-.88 IN-H80 -80.83
28.89 IN-H6 ' 733.80
95. F 35.
70.8 FPS 81.4
1142. 80-IN .737
1820/30. SCFH 5lSio.
2008713. ACFH 56711.
100.3 100.3
1 1 *t> 1 / .6
,364 LB/HR .16
1.5 1.5
< .0001 GR/D8CF* .273
.031 LB/HR .01
5.0 5.0
.0004 GR/DSCF* .909
!,,,.„„__, ,.,,j,, ^jjj LB/HR ': . " ' "' '-'•.."•••
24.1 24.1
.498 LB/MR .23




MM-HG
MM-H20
MM-H6
MRS
80-M
SCMrt
ACMH
-

KG/MR

M6/08CM
KG/MR
: ^^.-.s-, ,-
KG/D8CM
f

KG/HR





JS


.1

"1
;;











; *

-------
           EXAMPLE  PARTICULATE CALCULATIONS TEST NO. B3P-1


                 BAQHOUSE  N0*3 OUTLET
                                AV


     VMSTD •  (17.647  •  VM *  Y • (PB * PM / 13.6))  / (TM * 460.)
                17,647  •    203.493 • 1.016 * (  tS.«S * 6.797 / 13.6)
     VMSTD « ••**•*•*«**••»-•»••-•••••••—«.•-•.••..•.•-•—•——— i
                                                                    144.318 08CP
                                      * 460.J
                  ..,

     VOLUME Of NATEft  VAPflfc At STANOAfcO CONDITIONS
     VMC *  .04707  *  VLC


     VNC •  .04707  *    44.  •   2.OS SCP
     PERCENT MOISTURE  IN §TACK 6A3


     BNO »  (100.  *  VNC)  / (VMSTD » VNC)
 >
 I
               '100.  *    2. Of
         » ••,
                              . OS
 -J   MOLE FRACTION  OP DRT STACK BAS

...	MU K  (lpo>  m  g||U]  ; |>
-------
 STACK 6AS VELOCITY AT STACK CONDITIONS

 DELP * SUM.  OF THE 30RT(VH « (TS «• 460.))
 VS * 85.49 * CP * DELP / (SORT(MMS * PS) * PNTS)    ''

 V5 * 83 • 4^ * L  »fll "*L *" Tfift* 149 f (StiRT( 26 *7c • ?o •>6* J  *  27 •T   TO• IT FP3
 STACK CAS VOLUMETRIC PLOW AT STACK CONDITIONS

 03 « V5~* AS "* 3600/144	
 OS a   70.17 *  1142. 3600/144 •    2002713. ACPH
 3T ACK b*4 VutuMtTltlt ^LOw * I 41 AKu*Hl»
 OSSTD « 17.647 * OS • PS * (1. • (BNO/100)) / (TS • 460.)
           17,647 *    1002713. •  28.89 *(!.-( 1.04/100))
 OSSTD » ——..•—.•.——.——..———«.—*..——— •     1820730.  8CPH
                    T  »5.

 PERCENT ISOKINETIC

-ISO • (305.58*CTS»460;l)»(CO;002689«nC)»(VMtT«tPB»(PM/13.6^rrtT1<^0
-------
FIELD  DATA
;>' ' SAMPLING LOCATION
SAMPLE TYPE
OPERATOR
AMBIENT TEMP. (DEC. F)
STATIC PRESS. (IN. M20)
FILTER NUMBER (S)
PITOT TUBE COEFF!
THERM. NO.
,., .,.....,, ,. LEAKAVt """•"" "*i'WV".
METER CALIB. FACTOR
READ I RECORD DATA €*
CARTER-DAY BAGHOU8E OUT
LEAD
DAN FITZGERALD
80.
44.3?
-.42
0002303
42.00 .00
.82
127
lift1' ' 9.0 MINUTES
TRAVERSE SAMPLE CLOCK 6AS METER VELOCITY
POINT TIME TIME READING HEAD
CLOCK)
INIT 0 946
A-02 '* 16*0 •.'• 1024 :'l&
A-03 v 27.0 1033 J^
1 A-03 45^0 1051
M A-06 54.0 1100 '
y -ii^gw&MWT !w-WJ1-»3iW'V"H09«|p^
• A»06 72.0 1122 ?
A»09 61.0 1221
A-ll 99^0 1239
A-12 108.0 1248
A-14 126.0 1306
8-01 135.0 1323
B-62 1^4.0 U3i
8*03 153.0 1341
8-04 162.0 1350
8-06 160.0 1408
8-07 189.0 1417
8-08 198.0 1426 " 	
8-09 207.0 1445
B-10 216.0 1454
*, '" '"" ' B*ll " ' ' 425. V f',' 150S »?:,•".'
8*12 234.0 1512
8-13 243.0 1521
""" B-14 	 251.0 1530
TOTALS 251.0

923.854
941.100 .670
950.270 .720
95^.4lu .720
969.100 .770
976.860 .770
999.130 .920
10.385 1.100
" 21.325 	 1.000 ""
32.560 1.100
44.380 1.200
67.941 1.200
74.920 .400
Ad.uuO .4iO
89.650 .490
96.010 .580
115.494 .670
125.110 .730
''135.740 1.000
146.700 1.050
157.921 1.050
"169,310*""' 1*1UO
180.753 1.100
192.267 1.100
202.437 1.100
278.583



1" IWIHB "




ORIFICE PRESSURE
DIFFERENTIAL
1 \ i if * HBV 9 "^
DESIRED

""' WItF
2.34
2.51
2.50
2.67
2.67
3.19
3.62
3.46
3.61
4.15
K38
1.41
1.69
2.00
2.31
2.52
3.45
3.62
3.62
3.79
3^79
3.7T
ACTUAL

2.34
2.51
~2.50
2.67
2.67
3.19
3.62
3.46
3.61
4.15
i-. -»• « . i 5
4.15
1.36
1.41
1.69
2.00
%F* ' - C « 0 7
2.31
2.52
— —3.45--
3.62
3.62
"'" ' 3.79 '
3.79
3.79
3 . 79~




STACK
TEMP
EtttM.I1 >

"90.
90.
"92.
92.
92.
92.
92.
941
94.
94.
96.
	 96.~
97.
97.
96.
96.
96.
96.
'"""97;
97.
97.

RUN NUMBER CDL-1
PROBE L£N6TH 1 TYPE 5 FOOT GLASS 	 — •
NOZZLE 4-1171 I.D. .249
ASSUMED MOISTURE i.o
4«H**ut B0» HUFttR
METER BOX NUMBER FB6
METER HEAD DIFF. 1.53
PROBE HEATER SETTING 250.
HEATER BOX SETTING 250.
K FACTOR 1917.9
DRY GAS METER PUMP SAMPLE IMPINGER
TEMP VACUUM BOX TEMP TEMP
(utw.M ilh.Htt) ifrttt.P) ibCA.f) • -a"-.
INLET OUTLET

91! ss! 115 aso! 60!
93. 89. 3.0 250. 60.
99. 90. 	 3.0 250. 60. 	 ~~ 	
105. 92. 3.0 250. 60.
107. 94. 3.0 250. 62.
106. 96. '' S.O 250. 62!
107. 97. 1.5 250. 64.
~3 • ™ J • J • ^ C 3 v • DO «
96. 94. 3.5 250. 66.
102. 94. 4.0 . 250. 66.
110.- 96. 4.9 250. 66.
109. 99. 1.0 250. 66.
109. 99. I.O 250. 66.
110. 100. 1.0 250. 66.
110. 101. 1.5 250. 66.
107. 100. 2. 250. 66.
108. 100. 2. 250. 66.
109. 100. 3. 250. 66.
110. 100. 3. 250. 66.
105. 99. 3. 250. 66.
""" 108.' " tOO."' "" 3. '"•? '•Mi1' ' 67. " " '••' " r '?'
110. 100. 3. 250. 67.
110. 100. 3. 250. 67.
110. 100. 3.5 250. 67. 	 :



0
1
12
^
n!
1 7
1 I
1*
1^
2 ' _
tl
"
"
»•!
r.i
»o
st
19
1*
It
17
43
44
47
4*
HO
V t
• X
BJ
• 4
at
• 0
• *
• 4
• r
V*
M
71
74
7S

-------
           PARTICULATE FIELD DATA > RESULTS TABULATION



PLANT- NAME AND ADDRESS               TEST TEAM LEADER
fl l" '•:•-"
PRESTOLITE
TEST COL-

TEST D*T£
TB
• '• ' TF ' ' < • '
TT
NP
ON
CP
' "* ':**HT
JP* y U
VMSTD
VLC
VNC
BNO
FMO
PC02 ~
P02
,, ,._... , :.
PCO
PN2 ~"
MD
MM3
, MANCHESTER/ IONA ' ^
1 CARTER-DAY BAGHOUSE


TIME-START
Tine"Flnjaw ^ i • '-^ ••«$••
NET TIKE OF TiST, NINV* ^
NET SAMPLING POINTS
SAMPLING NOZZLE DIAMETER
PITOT TUBE COEFFICIENT
DROP
VOLUME OF DftT SAa 4AHl*Ltt)
AT METER CONDITIONS
VOLUME OF DRY CAS SAMPLED t
AT STANDARD CONDITIONS*
TOTAL H20 COLLECTED IN
VOLUME OF MATER VAPOR
At 9 t AND A Ad CQNDltlONS*
PERCENT MOISTURE BY VOLUME
MOLE FRACTION DRY 6AS
PtrtCtM liOi BY VOk.t OHi
PERCENT 02 BY VOL.r DRV
PERCENT CO BY VOL.» DRY
PERCENT N2 BY VOL.» DRY ~
MOLECULAR NT-DRY STACK GAS
MOLECULAR NT-STACK GAS
DAN FITZGERALD
OUT
ENGLISH UNITS
Ob/OB/Al
946
••"'"' ' ' 13»V" " , ' r' -'
291.0
26
.249 IN
.62
•T5i*--T 't#4^ 1W— n«w
2/6. Sa3 CU-^T
219.689 SCF
76.1
3.962 SCF
1.44
.966
.or
20.90
.00
T9.10
28.64
26.68
j ?• •% *«"-..' : si : • ". ''* :" ' ••• • • ••• ji ^
i *

METRIC UNITS ;°
06/08/ai
946
291.0
28 >!
,,i
.62 »
	 . . ,
'
>.o** CU-M
v : ' - *" "
6.997 SCM
76.1
•< -," -""v •- • "'• • * ' ' ', : ' '"*
.101 SCM
1.44
.966
.00 ...,,,
20.90
.00 «
79.10 	 ' ' ";.-
26.64 :;
28.66

-------
PB BAROMETRIC PRESSURE
PSI STATIC PRES OF STACK GAS
PS STACK PRES* AB8»
	 T* 	 "" 	 AVERAGE STACK TEMP ' ' '
VS AVG STACK GAS VELOCITY
A3 STACK ARtA s '*»'
tiidSTO STuCR PLOn H«It» DRY*
08 ACTUAL STACK PLOM RATE
ISO PERCENT I MR tilC Tt^^ •„ .
MN TOTAL Lt*U
M6. EPA 5
PMR TOTAL LEAD
tHtiSIUH HAIt
MN FILTERABLE PART,
CS ',,'" FILTERABLE PART* ^ ;>'-.
' r PMR FILTERABLE PART.
|Z. EMISSION RATE
* 60 Of • f, 19.41 1H.M«.

...T u ^,.,r,, ^.^.^r.

,,-^- ,,-,:.,^:,..,,,..e?..,^^,.,,

. ,*•' •,-•• ' .' *' •••''

''" , ' ^:,
28.57 IN-M6 725.68 MM-H6
-.42 IN-H20 -10.67 MM-H20
«0.54 IN-HG 724.09 HM-HG *
94, F 35. C i
53.1 FPS 16.2 MPS 7,
1305. 80-1N .894 SO-M ;"
It45^A4. 4CFH 46609. SCWH ri
1036109. ACFH 92052. ACMH ||
>•*•' I0i»5 ^ r ;:
ft " "1.3 1.3 %i
n.'f-i pfVtVl 
-------
       EXAMPLE PARTICIPATE CALCULATIONS TEST NO. CDL-1
            CARTER-DAT BAGHOUSE OUT
 VOLUME OF BUT 6A8 8AHPLEU AT ST*NPAHD
 VMSTO » (17.647 * VM * Y *  (PB * PH /  13.6)) /  (TM  *  «60.)
          VMSTO
           17.647 *   t*B.S83 *  .973 •  ( «.ST 4 Z.9«3  /  13.6)
                                                                     245.60S OSCF
                            101. 4 460. J
to
21
II
II
14
 VOLUME OF NATCH VAPOR AT ITANOAttO CONDITION!
 VHC • .04707 * VLC
                        /
 VNC • .04707 *   76. •   3.96 SCF
                                     r^*?, *;•'*''*"*•>-;
 PERCENT MOISTURE IN STACK CAS	"
 BNO » (100. • VNC) / (VM8TD * VNC)
                    100. *   3.91
         '8NO «•••*••— —••-•••
                               •»••  1.44 PERCENT
 MOLE FRACTION OF OUT STACK 6A8
                   •
     • (100. • BwO) / iOO.

 AVERAGE MOLECULAR NEI6HT OF DRV STACK GAS
 MO • (FC02 * .44) * (POf * ,3Z) *  (PNZ 4 PCO) *  »£•
"WT »~T  ;00»44/100) * (20.9*32/1007 * ((79.1*
 MOLECULAR NEI6HT OF STACK CAS
                - rBNO/IOO)) # 18. *  (BUD/100)
 MNS •  Z8.84* (1. -( 1.44/100)) * 18. *  ( 1.44/100) •   28.68

-------
          STACK CAS VELOCITY AT STACK CONDITIONS

          DELP • SUM. OP THE SORTCVH «  (TS *  460.))
          VS • SS.49 • tf • DEIP /  (SQRT(MNS • PS) • PNT8)

          V3 • 45.49 "*  J"8"2*  606.4611  ISuM( 26.68  «  28.51)   *24.  *~~S3.0T~
          STACK *A8 VOLUMETRIC H.O*  AT STACK CONDITIONS
          OS * »3 • AS•


          OS *   S3.07 *  13SS. 3600/144 •     16381S*.  ACFM
II
tl
i«         &(Atn bAS VOLUME Ifiid I"LOh  nl Stitfiij^kU Cunbl I iUNi

          OSSTO « 17.647 * 08 • M * (1.  •  (BNO/100))  /  (TS  * 460.)
                  '  17.647 t     1838149.  *   »O.S«  *  (1.  -  (  1.44/100))
          OSSTD * .—..—..•..*•...——•.•-..•..———.....—«..— •    164S984. SCfH
          WEHCENT ISOKINtTlC
          180
                 (30S.5S*(  »4.*460. ))•({«. 002669*    76.)+(   270. 5S3* .973*( 2S.97«(   2. 993/13. 6))/(  101.+460.)))
                                              251.  *      S3.07 «   2S.S4 *  .249 •  .249
          PARTICIPATE LOADINC ••  EPA  METHOD  S  (AT  STANDARD CONDITIONS)
• I
          C8 « 0.001 * MN *  13*43  /  VMSTO
               V*VV1
!!         PARTICULATE L88/HR •*  tPA  METHOD f

45
          PMR « C3 « OSSTD /  (15.43  t  433.6)	

          PMR «     .000 «     16459S4.  /  (15.43 «  453.6)  •	.02
IX,

14




?

-------
FIELD  DATA
SAMPLING LOCATION
	 ~ 	 SAMPLE TYPE "
OPERATOR
AMBIENT TEMP. (DEC. F)
u; .; ,:,,,,; ,,,,„. • BAR.pReSS.CIH.H6)
STATIC PRESS. (IN. H20)
FILTER NUMBER(S)
STACK INSIDE DIM. (IN)
PITOT TUBE COEFF.
THERM. NO. ,
CARTER-DAT OUTLET '
1VNM

LEAD M 12
REINERMANN
70.
*" "• W.77 ' "" •i"" : • 	 '-'• ' "" 	
-.42
0002161
42.
.62
127
•" METER CALIB. FACTOR ^973
READ « RECORD DATA EVERY 9.0
TRAVERSE SAMPLE CLOCK GAS METER
POINT TIME TIME READING
CLOCK)
INIT 0 607
B-13 16.0 625
B-12 27.0 634
B-ll ' 36.0 " 843
>P 8-10 45.0 652
1 B-09 54.0 901
£ B-07 72.0 919
8-06 61.0 928
" 	 B-05 90.0 ' 937
B-04 99.0 946
B-03 106.0 955
•••" nl "i" B»02'"'T' 11 1.0' <"""! Of • "*'-','•
B-01 126.0 1034
A-14 135.0 1055
-12 153^0 1113
-11 162.0 1122
t ""•••'"• 	 • «10 """171.0 "" 1131 8'"fTV
-09 180.0 1232
-06 189.0 1241
*07 198.0 1250
-06 207.0 1259
-05 216.0 1308
• 04 225. V "" 1317 •",! ""
-03 234.0 1326
-02 243.0 1335
_____ 	 €iQ1 	 252.o 	 IJ4* 	
TOTALS 252.0

VCU.M»f
272.674
295.774
307.146
T18.675~
330.440
341.626
362.341
371.476
~sso.t>or~
366.315
396.242
404.100 "
411.577
423.125
446^473
456.115
469«>93'
461.156
492.685
~30ZT803
312.163
521.733
'530,925
540.233
549.227
557.796
284.922

00 .00
CFH • *..
MINUTES
VELOCITY
HEAD
"lift. MO) '

1.100
.050
.050
	 .100 "
.100
.000
.740
.650
.580
.540
.500
'•"• *»500
.440
1.100
lllOO
1.100
** ' ' 1.100
1.200
.990
.630
.710
.720
' ' ' 	 ".6TO " '
.660
.630
....
4
PHTE
RUN NUMBER

PROBE LtNCiM » lift
NOZZLE 4-1171 I.D.
ASSUMED MOISTURE
aftpfr'LE BOx
METER BOX
HETER HEAD
NUPBCK
NUMBER
OIFF.
C FACTOR
PROBE HEATER SETTING
HEATER BOX SETTING
Ilf.M.
CDL-2
5 FT 6LASS
.249
1.5
FB6
1.53
.92
250.
250.


K
rr

ORIFICE PRESSURE
DIFFERENTIAL
T tin.
DESIRED

3.86
3.86
4.10
4.10
3.68
.*»
2.68
2.35
' 2.06
1.95
1.79
.79
1.56
4.10
4^10
4.10
4.40
3.60
" 3.10
2.60
2.60
2.50
2.30
~2.ro
3.4-3
niuj
ACTUAL

3.86
3.66
~47TO"
4.10
3.66
2.66
2.35
2~;08
.95
.79
.58
.10
.10
.10
.10
.40
3.60
3.10
2.60
2.60
'1 ' "' '2.40
2.50
2.30
2.I
.0
.0
"""' '!'«9 .'*'""
.0
.0
.0 "
.0
.0
" ,Jj'»""
3.0
3.0
	 y^(r-
•J.9

tl
223.
240.
-esu.
250.
225.
Vii
840.
230.
240V
230.
230.
240.
240.
240.
245.
245.
(40? ' "
240.
245.
*30.
250.
250.
•3tf
*30.
243.
§40*
IMPINGER
TEMP
tUEC.F) 	 '


?•
* A. • •• '•• , ••%
34.
50. i
50.
SO.
49.
49, ~: ' .. .' , |... • .
51.
51.
31. ' "~
52.
52.
30. 	 - ' "— "?
50.
55.
30.
30.
30.
30. '.-' "' 	 ' 	 "••'M-jjujj
30.
50.
0.
0.
0.
'35. • - - ' ' '?"!'..'4f
30.
55.
30. . '


~






-------
           PARTICULATE FIELD DATA I RESULTS TABULATION



PLANT* NAME AND ADDRESS               TEST TEAM LEADER
PRESTOLITE
	 	 '(
MANCHESTER IOWA
REINERMANN
	 ^ 	 • •"••" 	 T 	 7- 	 — 	 	 	 	 	 	 	 	 T>.
TEST CDL-2 CARTER-DAY OUTLET •

ttii uAffe
TB
\ • * r ' •"*"*•
TT
NP
DN
CP *
' ' •
I-1
VMStO
VLC
VNC
BNQ
FMO
PC02
PCO
MD
MM8

TIME-START
NET TIME Of TtSt, :Nt*!!^r '
NET SAMPLING POINTS
SAMPLING NOZZLE DIAMETER
PITOT TUBE COEFFICIENT
DROP
VOLUME Or DRY CAS SAMPLED '
AT METER CONDITIONS
VOLUME OP DRY CAS SAMPLED
AT STANDARD CONDITIONS"
TOTAL H20 COLLECTED IN
IMPlNfERS AND SILICA CCUfNt<
VOLUME OF WATER VAPOR
AT STANDARD CONDITIONS"
PERCENT MOISTURE BY VOLUME
MOLE FRACTION DRY CAS
PERCENT C02 BY VOL.* DRY
PERCENT 02 BY V0L.» DRY
PERCENT CO BY V6t,i. DRY
PERCENT N2 bf VOL.* DRV
MOLECULAR NT-DRY STACK GAS
MOLECULAR NT-STACK CAS
ENGLISH UNITS
Ob/10/81
607
292.0
26
.249 IN •
.62
*TV'' "<9U1 IRPMU
264.922 CU*FT
254.367 SCP
171.2
B.09S scr
3.09
.970
.00
20.90
.60
T9.10 	
26.84
16.51
METRIC UNITS |°
Ob/10/Bl - • • rj
807 ;•
292.0 • - ;;
, "„,. . , , 	 i
-*•' ' ' : ,,
6.3 MM ;;
.82
12

8.066 CU"M ,,
7.299 SON ;;
171.2
"••:••" • ' ' •-••*• 	 v>: f-* ' '
.226 sen ;;
3.05
*. ••1J* ' , •"-•'«(•. k ' • • \
.00
20.90
. .- ., , ^ , ,,. , ...,.w,.,:,^.. - . .. -7,. ...,T*
79.10
26.84 ,
••-• 	 • • """ ' > 	 r*:1-*1 T • - 	 -•--,-. ;!.„
".»» ;:

-------
PB . BAROMETRIC PRESSURE 28
PSI STATIC PRES OF STACK GAS
PS STACK PRES, ABS.
»
TS AVERAGE STACK TIMP 90
VS AVG STACK GAS VELOCITY 52
AS STACK AREA
1385
OSSTO STACK FLOW RATE, DRT* 1624339
03 ACTUAL STACK FLOH RATE 1817865
ISO PERCENT ISOKINETIC
. MN '"" TOTAL LEAD
* MG. EPA 5
t" CO • TDTML LCHU . Up*-"*
' PMR TOTAL LEAD
EMISSION RATE
MN FILTERABLE PART.
'•""""" " '"T 	 MS, EP« 3 '• '"'
>L CS FILTERABLE PART.
CK PMR FILTERABLE PART.
EMISSION RATE
* 68 DEC F, 29.92 IN»HG
»•»
•• • ' ' . ii
1

13


•
.77 IN-HG
.42 IN-H20
,»4 IN-HG
. K
.5 FPS
. 80-IN
. " SCFH
. ACFH
.9
.0
.014 LB/HR
.7
.0008 8R/08CF*
.191 LB/HR
'
730.76 MM-H6
-10.67 MM-H20
t*9.9T MM-HG ji. '
u.o OPS ;
' .894 9Q-M ;°
459*6. 8CMM ' - n
51476. ACMH \\
106.9
1.0
.01 KG/MR
13.7 ;;
"" 	 V '" 	 * .;---•'- ,;y.- ".r- -:•--- T---- -- ' ' ' - 'If
1.887 H6/08CM ';;
.09 K8/HR '•
• " (-. : ; • ' '. : '*-- ^ LJ1I jf.,- » > 5- -i. .. - . -, , if?

: •'





«

!*

t 6-
2
1
A
6

-------
      EXAMPLE PARTICIPATE CALCULATIONS  TEST  NO.  COL-2

            CARTER-DAY OUTLET
VOLUME Of b*T 60S SAHPtEO  AT STANDARD  CONDITIONS	

VMSTO • (17.647 • VM *  T *  (PB  »  PM  /  13.6))  /  (TM * 460.)
VM8TD
          17.647 *   114.922 «   «97S  *  (  28.77  * 3.124 / 13.6)
          **»*-•*•.•••••...•.••••—...-—*-......-—.-.—
           , - j — 93.  *  460.) ----- - -- —~  ~
356.367 08CP
VOLUME-OP MATER VAPOR  AT. WAND ARC  CONDITIONS
 	,	:S3L-L-:..^ •;	
VWC • .04707 *  171. •    8.06  SCF
PERCENT MOISTURE  IK  STACK  CAS  '	

BNO • (100. * VMC) / (VMSTD  *  VNC)
•NO •
          too,
           256.36T »—rrof
                                  »   3.05  PERCENT
    « (100. • 8HO) /  100.

          100. •   3.0
               loo. ,-.••**
AVERAGE MOLECULAR HEIGHT  OP  DRY  STACK CAS
MO • (PC02 •  .44) «  CCOt *  .32)  * (Pit * PCO) » .20

MB » t—.oot44/ioo)  »"t2o;tr32rioo)  » ((79.i» ,irr-«-
MOLECULAR NEI6HT OP  ITWK  tAl

   ~-Tr~mr~rTI."'"- (BRO/100))  * 18.  *
MN8 •  28.84*  (1. -(  3.09/100))  » 18. * ( 3.05/100) •   28.51

-------
 STACK GAS VELOCITY AT STACK CONDITIONS
             /


 DELP » SUM. Of THE 8QRT(VH * (TS * 460,))
                                                                                                                                   TTA
 VS » 65.49 * CP • OELP / (SQRT(MMS * PS) * PNTS)
vS * 05.
              .82 *
                                                                  52.48 fPs"
 STACK CAS VOLUMETRIC PLON AT STACK CONDITIONS



~0~S * VS * AS * 3600/144



 OS •   52.48 *  1365. 3600/144 «    1617865. ACFH
 STACK CAS VOLUMETRIC H.U* 'At STANDAHO CUNtrrmmS	


 OSSTD • 17.647 * OS • PS * (1. - (BNO/100)) / (TS » 460.)
          17.647 «    1617665. •  28.74 *(!.•( 3.OS/100))

8SSTD • «...•...•—«.—•—-•—.—....—.—•—•—«.— »
                                                                  1624339. 8CPH
                           * 460TT
 PERCENT ISOK1NETIC
                                                        l3*6) ) /



        (305.58*(  90.«460.))*((0.002669«  171.)*(  264.922* .973*( 26.77«(   3.129/13.6))/(  93.4460.)))
                                    2SX. «     52.46 *   28.74 *  .249 *  .249
 PARTICIPATE LOADING " EPA METHOD 5 (AT STANDARD CONDITIONS)
 C8 « 0.001  * MN • 15.43 / VM8TO


~CTT( 0.001  *	t.O * 15.43 /	256.367
                                               .000 CB/DSCF
 PARTICULATE LBS/HK *« IPA METHOD 5
PMR
      ti • u^alO 7 iia.43 "453.0)


          .000 •    1624339. / (15.43 • 453.6) »
                                                       .01

-------
                                                                 in
FIELD  DATA
f


•
3
t
T
f
I*
JO
XI
2
1
4
7
0
IX
3
4
t
7
0
1
2
41
44
1
9
»
0
2
IS
V
f ' " ,



SAMPLING LOCATION
innfut tVPE
OPERATOR
AMBIENT TEMP. (DEC. F)
STATIC PRESS* (IN.H20)
FILTER NUMBER (8)
5T»tR IwSIOl Dln.llH)
PITOT TUBE COEFF.
THERM. NO.
CARTER DAY OUTLET
LEAD M12
REINERMANN
68.
' . • It. to • -T •* •"•• •'. '
-.42
0002249
42.
.82
133
METER CALIB. FACTOR .973
READ • RECORD DATA EVERY 9.0
TRAVERSE SAMPLE CLOCK GAS METER
POINT TIME TIME READING

INIT
8-13
B-12
'$* B-ll
1 B-10
,, 9 v »
8-07
B-06
8-05
-04
-OS
-01
-14
7 	 -is
-12
-11
5r •?"—""' -iv
-08
'"" 	 "' *07
-06
-05
•03
-02
A-Ol
TOTALS
AVERAGE'

0 743
- 18.0 801
27.0 810
	 36.0' 819 	
45.0 828
54.0 837
"• '72% ''""ess ^T"r?
81.0 904
90.0 ' 	 913 "'
99.0 922
108.0 931
" 126.0 949
135.0 1020
1*4.0 1024
153.0 1038
162.0 1047
•^r ifi.v7"^"1 ivSw s ''wj,
180.0 1105
189.0 1114
" 198.0 1123 "' "*"'
207.0 1225
216.0 1234
234.0 1232 •'." '
243.0 1301
252.0 1310
232.0


560.019
580.961
591.111
602.999
614.727
625.463
645.060
653.864
"6*27135"
670.058
677.756
691.708
703.573
715.601
727.653
739.693
763*502
775*056
"785.167
794.764
804.102
822^639
831.513
839.773
279.734

vu .vu
trn • ib*
MINUTES
VELOCITY
HEAD


.950
.950
••"• - T.ioo"
1.100
.950
. 63v
.700
.630
.560
.500
.470
.350
1.200
1.200
1.200
1.200
%$£** * 1 »CWW
1.100
1*100
	 .830"
.770
.730
.680
.630
"".550~
''t'"" "fPf"
RUN NUMBER
PROBE LENGTH 1 lYPt
NOZZLE 4-1171 I.D.
ASSUMED MOISTURE
METER BOX
METER HEAD
NUMBER
OIFF.
CDL-3 «
5 FT GLASS - - "" •
.249
1.5
FB6
1.53

t mtlUN ,v< n
PROBE HEATER SETTING 250. "
HEATER BOX SETTING 250. '|
!!
ORIFICE PRESSURE
DIFFERENTIAL
liw.f
DESIRED

. a.ci
3.42
3.42
4^10
3.42
3,10
2.53
2.25
ileo
1.69
1.26
4.40
4l40
4.40
4.10
4.10
3.00
2.80
2.60
2.50
2.30
	 2.0T)

nvi i
ACTUAL

3.42
3.42
~4.IO ~
4.10
3.42
3.10
2.53
2.25
2.00"
1.80
1.69
1.26
4.40
	 47* 0~
4.40
4.40
4.10
4.10
1 ' 3.00
2.80
2.60
2.30
2.30
2.00'
- •?'«,« 5.««
STACK
TEMP


at*
88.
89.
901
90.
91.
91.
92l
92.
91.
91.
93l
95.
93.
96.
'" 96.
97.
98.
48.
97.
"98.

DRY GAS METER
TEMP
iucw.rV
INLET OUTLET

72. 63.
80. 66.
83. —"TO.
87. 72.
87. 73.
91. 77.
92. 79.
93. 	 "81.
94. 82.
95. 82.
95. 84.
88. 85.
90. 85.
94. 86.
97. 87.
'*
100. 90.
101. 90.
102. 92.
96. 93.
100. 94.
108. 46.
110. 96.
110. 98.
PUMP
VACUUM


•9
8.0
8.0
10.0
10.5
9.0
t.o
6.0
5.0
5.0
4.0
11.0
11.0
11.0
11.0
i • V
10.
9.
T.
5.
5.
5.
5.
4VO
SAMPLE
BOX TEMP


250.
243.
230.
260.
240.
230.
230.
"24U.
273.
260.
230.
230.
"" "230.
233.
250.
fjj, w
235.
250.
'" 233.
250.
250.
•30 1
230.
230.

IMPIN6ER »
TEMP "
fVBI.F) ' " "• • ! „
I"

• ' .- .-,'-''- »' IT,,
30.
so. ;;
50. ,-.
48.
48.
30 !
*•• «
* I •
51.
31.
34. «•«
30. 1
30. •„
55.
JO.
55.
30.
33.
50.
50. i
35.
50.
30.
•Ifl, --• ' ' 'VI':

-------
           PARTICIPATE FIELD DATA B RESULTS TABULATION
PLANT- NAME AND ADDRESS
TEST TEAM LEADER
•-• - '-"•' : • * 	 ••••-"• ;-f •""•
> PRE8TOLITE MANCHESTER, IOWA
. TEST

10 TEST
11 TB
i. TF
!. TT
', NP
a. ON
CP
, 	
' **•" PW 'i'^'
M
NJ
O
VMSTD
VLC
; vwc
BMO
FMO
PC02
P02
PCO
PN2 ~
MO
HNS
CDL-3 CARTER DAY OUTLET
' >•*?•">• ' • -i> . •
DATE
TIME-START
NET TIME OF TEST, «!«» 4V
NET SAMPLING POINTS
SAMPLING NOZZLE DIAMETER
PITOT TUBE COEFFICIENT
' ' DROP
VOLUME OF DRT GAS SAMPLED"
AT METER CONDITIONS
VOLUME OF DRY 6AS SAMPLED
AT STANDARD CdNUltlUNO*
TOTAL H20 COLLECTED IN
VOLUME OF WATER VAPOR
AT STANDARD COnditliiNS*
PERCENT MOISTURE BY VOLUME
MOLE FRACTION DRY GAS
PERCENT COS BY VOL. i DRY
PERCENT 02 BY VOL., DRV
PERCENT CO BY VOL., DRY
	 PERCENT N2 BT VOL.. DRY
MOLECULAR WT-DRY STACK GAS
MOLECULAR WT-STACK CAS
REINERMANN

*"
ENGLISH UNITS
06/11/81
743
13}V
232.0
28
, .249 IN
.82
•>_ •- «;*S»B» iMHW
279.754 CU-FT
233.824 SCF
196.9
9.268 SCF
3.30
.963
.00
20.90
.00
79.10
28.84
28.46
•I-..-; .-,.•'. •• • • H t

METRIC UNITS ',°
06/11/81
743
1J10 • • „ *
232.0 : •£ ""* •,
28 l't
6.3 MM H
.82
i ' "
t.iii CU-M ]
7.244 SCM ;;
196.9
.262 SCM ;;
3.50
.963 " '''r . ' "<•„
.00 j«i
20.90
.00
79.15 ""• " 	 ' " - 	 	 ~ •- -•-•• ' • • - - - - ^
28.84 ^ ;;
as. 46 ;;

-------
PB BAROMETRIC PRESSURE
P8I STATIC PRES OP STACK
1 PS STACK PRtB* ABS.V
28.98 IN-M6 736.09 MM-MG
i
GAS ».«2 IN-H20 -10.67 HM-H20
'' ' 28.95 IN-H6 739.31 MM-MG
4 '••••"1TS 	 AVERAGE STACK TEMP1* «»3. ' F 54. t
! VS AV6 STACK BAS VELOCITT 51.9 FPS 15.8 MP8
AS STACK AREA
* • ••-' JLiJ-HJ.. Ill ML. «1 JX I.1J11
1385. SO-IM .894 SO-M
10 U99TD 3T*tH Ft»UN rtHIEf UHT* lOUi^^l. 9CFH 4337^. 9CWH
!i OS ACTUAL STACK FLOW RATE 1798152. ACFH 50918. ACMH
!! ISO :. " PERCENT ISOKtNtttt^^^^../ / 106*1 108.1 ..,,,.,,,. ....
i. HN YUT*L LE*b ... •* .4
.7 MO. EPA 5
tt '* '
H PMR "::;'^: tOTAL LEAD ' ?!,Vki
it tMl99lON H*ft
" MN FILTERABLE PART.
M!*^*..- ' 9-^^S'**HIJ wi»'ftFi--f -" "Ui(i|p
" CB k FILTERABLE >ARTi ; .•
"t 1 PMR FILTERABLE PART.
„ ^J EMISSION HATE
,i • '• * 68 OEB f» t^t*tt IN*Nit
.012 LB/MR .01 K6/HR
6.0 8.0
/, ;; .0005 GR/08CF* 1.104 M6/08CM
.110 LB/HR .05 KG/MR
r*?":"': :-r-:-^1-- : -: K'^--!I -^- -^•- •-*-***-«" -
»
»• ..,'.. 'Vw-i "V

•o
•< *
44 ; ' •• ' '; *'; /•,. « • '••;-. -. *". -: •
4t ^ ,
4«
47
« . .. ..,.....„ ,«.^ . ..fn*T.'^^.
• a
•»
"
V

T^7.^""^"" " -- • — ^ " >•*•> -^"wr^r» " • "'^
•-
"'•'''"'IpWflf?1?1'1 '•' '"^fW*UJ '''I?:*1* " '.•• -?*•-. v. .^;-j- '"• ' ; v w,tv ••;w»T^'": ''* fsjT'W'!'.^'. - .-•; T • "''• "' I^-
N















-------
                EXAMPLE  PARTICIPATE  CALCULATIONS TEST  NO.  CDL-3

                     CARTER DAT  OUTLET                                                                                                         *"
                 OP~DRT  CAS  SAMPLED AT  sTANornRtrctrTOmoNS         ~~

          VMSTO  « (17.647  •  VM • T • (PB * PM / 13.6))  /  (TM * 460.)
                    17.647  *    179.754 *  .973 * (  28.98  *  3.061  /  13.6)
          VMSTO  «......—»••-..-—•—•.-.—————••——•——  m    255.824 D8CF
                                                                —       ,      -- - -	
          VOLUME  OP  HATER  VAPOH AT STANDARD CONDITIONS
                       *  VLC"

          VNC  •  .04707  *   197.  *    9.27 8CF
  	'PERCENT  MOISTURE  IN  STACK  CAS	
13
          BNO  «  (100.  •  VNC) / (VMSTO * VMC)
                    100.  •    9,27
          BNO  »  .-••——.»—•..—....... •.•  3.SO PERCENT
                             *
    10     MOLE  FRACTION  OP  DRY  STACK  SAS
          AVERAGE  MOLECULAR  HEIGHT  OP  DRY  STACK  GAS
                                     .
          MO  »  (Pe02  *  .44)  »  CP02  *  .32)  *  (PN2  *  PCO)  *  .88

          HD  » T — ;W>*44/|Qa)  *  C20.9»32/100)  *  (CT9.1*  ;01 ^ 28/100
          MOLECULAR  MEIGHT  OP  STACK  6A8

       —MIS  r MD-*-err ^~«wo/rao))  * rsr»  IBHO/IODI	 	

          MMS  *   28.84*  (1.  >( 3.50/100))  * 18.  *  (  3.50/100) •    28.46

-------
       STACK 6*$ VELOCITY  AT  STACK CONDITIONS

       DELf» • SUM. OF THE  SORT(VH *  (T8 * 460.))
       VS * «9.49 * CP • OELP /  (SQRTfNNS • PS) • PNTS)

      -V8~Tr-g5.49 »—^m—595.189 / "(SORT ( 88.48 « "28.951—«"  28.  »--"5t,
       STACK 6A8 VOLUMETRIC PLOW  AT STUCK CONDITIONS

       tit * VS '• As A
       08 «   91.42 *  1385.  36*0/144 •     1796152.  ACPM
is*
NJ
U)
       SUCH 608 VOLUME>R1C PLUM  M  8TMPAHO

       OS8TD « 17.64T « OS «  PS » (1. "  (BHO/100))  /  (T8  *  460.)
                                                                                                  Mf:
     :-\~%f----  •-, i •   .-•
          |f«647 «
OSSTD « •*-•....»•.
 1790152.  ft   21.95  •(!.-(  3.50/100))
....*..*..*........................... •
                                                                         1601551. SCfH
PE^CINT ISOKINET1C

180 « (
       (305.58*(  93.*460.))*((0. 002669*  197. )*(  279.754*  .973M
                                                                                     3.061/i3.6))/C  88.»460.)))
                                           252.
                                              51.92 *   28.95  •   .249  •   .249
       PARTICULATE LOAOIN6  ••  EPA  METHOD  5  (AT  STANDARD  CONDITIONS)
                          ,
CS * 9.001 « MN * 15«4J / VM8TO

                  ^9 • 15.43 i
          «  .
                                                       .
       PARTICULATC L8S/HR ••  tf«  MlTMOO
PMR •
                  HSo

                  .000  *
              TO / (15,43
 1602551.  /  (15.43.*  453.6)
HF"
                                 .01
                                                                                                                                        ~™t

-------

f" ¥,'• " •'-;,'
_ _
•

• '- -"V

PLANT
SAMPLING LOCATION
SAMPLE TYPE
OPERATOR
AMBIENT TEMP. (DEC. F
BAR. PRESS. (IN. HG)
STATIC PRESS. (IN. H2
FILTER NUMBER(S)
STACK INSIDE DIM. (I
PtTOT TUBE CqF_FF,
THERM. NO.
LEAKA6E
METER CALIB. FACTOR
READ ft RECORD DATA
TRAVERSE SAMPLE CLOCK
" • POINT
NO.

TIMI TIME '
IMIN.) (24-HR
CLOCK)


PRESTOLITE, MAN
CARTER-DAY BAGH
PARTICULATE
DAN FITZGERALD
) 80.
28.57
0) -.42
00002255
N) 42.00 .00
.84
174
.000 CFM « 4.
1.018
EVERT 9.0 MINUTES
GAS METER VELOCITY
READING HEAD
(CU.FT.) (IN.H20)


CHESTER,
QUSE OUT

E1EJ.D_J)ATA
IONA







DATE
RUN NUMBER
PROBE LENGTH ft TYPE
NOZZLE 4-102: I.D.
ASSUMED MOISTURE
SAMPLE BOX NUMBER
METER BOX NUMBER


06/08/81 *
CDP-1
5 FOOT GLASS ;
1.0
FB3
METE« MEAD OIFF. 1.94
PROBE HEATER SETTING 250.
0 IN.H6
ORIFICE
DIFFE
(IN.
DESIRED

_P.K£13yjE_
RENTIAL
H20) (
ACTUAL

JLTACH
DEG.F)

HEATER BOX SETTING
K FACTOR
DRY GAS METER PUMP
TEMP ?ACUUfT^1
(OEG.F) (IN.HG)
IKLET OUTLET
250.
2471.
SAMPLE
ITO TEMP
(DEG.F)



:„.--, • • - |
2 Z"
IMPINGER ',1
TEMP " "
(DEG.F)

I*
"? '- 8-13
» M B-12
£ B-ll
10 •*• B-10
' B-09
B-08
B-07
B-06
B-05
B-04
B-03
B-02
B-01
•14
•13
-12
•10
•09
-08
-07
-06
-05
-04
-03
-02
•01
TOTALS
AVERAGE
* '•• d ^ •' »«ih" ,
9.0 957
18.0 1926
27.0 1035
36.0 1044
45.0 1053
54.0 ^ 1102 ;
63.0 1111
72.0 1120
81. 1129
90. 1228
99. 1237
108. 1246
117. 1255
126.0 1304
135.0 1321
144.0 1330
	 >53aO 	 133? 	
162.0 1348
171.0 1357
180.0 1406
189.0 1415
198.0 1424
207.0 1443
216.0 1452
225.0 1501
234.0 1510
243.0 1519
251.0 1528
251.0
<• 82.139
92.640 .100
103.100 . jilOO
113.655 .100
123.850 .000
134.020 .000
144.225 .000
154.120 .920
163.265 .780
171.800 .680
179.895 .600
187.935 .600
199.630 .550
202.900 .480
209.749 .400
220.370 1.100
231.280 1.100
242.510 1.100
253.344 1.100
264.000 1.100
274.891 1.100
285.550 1.050
295.560 .890
305.027 .840
' 314.760 .870
324.304 .830
333.770 .810
342.901 .720
350.815 .720
268.680
4.87
4.87
4.86
4.42
4.42
4.42
4.07
3.01
2.64
2.66
2.43
2.12
. 1.77
.85
.85
.84
.85
.86
.86
.64
3.93
3.71
3.85
3.66
3.57
3.18
3.18
3.89
.87
	 _. .87
.86
.42
.42
.42
.07
3.01
2.64
2.66
2.43
2.12
_.. 1.77
.85
.85
.84
.85
.86
.86
.64
.93
.71
.85
.66
.57
.18
.18
3.89
98.
.. «..
99.
99.
99.
99.
99.
99.
99.
101.
98.
99.
99.
99,
100.
100.
LP±._
100.
99.
99.
99.
99.
"«_
99.
100.
too.
100.
99.
99.
80. 78. 2.
_89, _ 79. 2.
90. 82. 2.
99. 83. 2.
101. 85. 2.
103. "•••'- 88. ^1.1""
104. 89. 2.
105, 90. 2,0
105. 91. 2.0
106. 92. 2.0
95. 91. 1.5
100. ^ 91. 1.5
103. 91. 1.5
104, 92. 1.0
104. 94. 2.5
107. 94. 2.5
110. 95. 3.0
111. 96. 2.5
11. 96. 2.5
10. 98. 2.5
10. 97. 2.5
10. 97. 2.0
11. 97. 2.0
106. 98. 2.*
109. 98. 2.0
111. 100. 2.0
112. 100. 2.0
112. 100. 2.0
104. 92. 2.2
250.
290»
250.
250.'
250.
150.
250.
250.
"250.
250.
250.
290.
250.
250.
250.
255.
255.
255.
255.
255.
255.
255.
255.
25S.
255.
255,
255.
255.
252.
60.
60.
60.
60. ;;
60.
-*Q. '
60.
60.
60.
60.
62.
64.
64. j
64. !
66 • ;:!
66.
66. ,
r 66. •-••; • - •
66. "
66. !«!>
66. s'
66.
66.
' 66. T ?
66.
66, ^i
66.
66.
64. .'.

-------
PARTICULATE FIELD DATA I
fPVW'.^irtrf. NAME AND ADDRESS *•"" '; ";• ' '"*•
PRESTOLITE* MANCHESTER* IONA
TEST CDP-1 CARTER-DAY BABHOUSE

TE8T DATE
TF TIME-FINISH ' ' • H t,wfc<
ff NET TIME OF TEST, HIN^X
NP NET SAMPLING POINTS ...j. 1.
Y METER CALIBRATION FACTOR
ON SAMPLING NOZZLE DIAMETER
CP PITOT TUBE COEFFICIENT
| PM AVERAGE ORIFICE PRESSURE
j&* , DROP
"T" 	 " 	 '
£ VM VOLUME OF DRY GAS SAMPLED
in AT METER CONDITIONS
TM AVERAGE GAS METER TEMP *
.
VMSTO VOLUME OF DRY GAS SAMPLED
AT STANDARD CONDITIONS*
RESULTS TABULATION
^ ^Tf Sf •ftUN LEADER *
DAN FITEGERALD
OUT
ENGLISH UNITS
06/08/81
1928
251.0
28
1*018
.250 IN
.84
'l 3.89 IN-H20
i
268.680 CU-FT
"" 98.2 F
249.909 SCF
?"""7' VtB4"vl> ' TOTAL H20 COLLECTED lit V-'- - •!,* "- T
IMPINGERS AND SILICA GELrML.
VNC VOLUME OF MATER VAPOR
AT STANDARD CONDITIONS*
^^f^-nO "7 PERCENT MOISTURE BY VOLUM1
FMO MOLE FRACTION DRY GAS
PC02 PERCENT COt Bt VOL., DRY
PCO PERCENT CO BY VOL., DRV
PN2 PERCENT N2 BY VOL., DRY
3.836 SCF
*985
.00
VW9+ ' •
79.10
^~ ° MO ' MOLECULKR WT*ORT STACK GAS'' ' ' I8-»B4
MW8 MOLECULAR WT-8TACK GAS 28*67
I


METRIC UNITS ..... . . . il
il
06/08/81 *
^ ' " ""* ' 'I'-.J """ " " :
251.0 ;
28 «
1.018 ;
6.4 MM •
.84 :
9B.7 MM«H20 * «
••'•i- i «i
H
7.608 CU-M \H
36.8 C ''"'.'' ' •.-»...- ...-,. • ^:
7.065 SCM j
2
.104 SCM
4
1
.985 I*
.00 ;
• 4
•*•'. ' *
.00 i
• *
79.10 :
'• • 78*84 >,-^ ••• ' f-- JF^- •-«-.• ,-i • ' "
28,67 !•*

-------
                                                                                                                / 7' /
PB
I1 : P3I
PS
TS
V8
AS
03STO
OS
{80
MN
CS
PMR
'•• ': MN ' ; '
(i PMR
to --'" -
Ch
L- MN
CS
PMR
MN
CS
PMR
«' MN
CS
PMR
MN
BAROMETRIC PRESSURE
STATIC PRE8 OF STACK GA8
STACK PRC3, ABS.
AVERAGE STACK TEMP
AVG STACK 6A8 VELOCITY
STACK AREA
STACK FLOM RATCr DRV*
ACTUAL STACK FLOX MATE
PERCENT laOKtNETlC
FILTERABLE LEAD
MG. EPA 5
FILTERABLE LEAD
FILTERABLE LEAD
EMISSION RATE
CONO. LEAD <-r- ' •":*•''.
MG. EPA 5
COND. LEAD
COND. LEAD
EMISSION Mte ' ; ;i ;
FILTERABLE PART
MG. EPA 5
FILTERABLE PART
FILTERABLE PART
EMISSION RATE
COND. INORGANIC
MG. EPA 5
COND. INORGANIC
COND. INORGANIC
EMISSION RATE
CONOESABLE Oft«*Nie
MG. EPA 5
CONOESABLE ORGANIC
CONOESABLE ORGANIC
EMISSION RATE
TOTAL PARTICULATE
28.57 IN-HG
•.42 IN-H20
28.54 JN-HO
99. F
55.2 FP8
1385,. SO-IN
1696562. SCFH
1*118*3. ACFH
'*.«
1.4
.0001 GR/DSCF*
.021 LB/HR
"','••'
.0000 GR/DSCF*
.000 LB/HR
13,7
.0006 GR/DSCF*
.205 LB/HR
5.8
JJ-Jt'. '
.0004 OR/OSCF*
.087 LB/HR
S.7
.0002 GR/DSCF*
.055 LB/HR

725.68 MM-HG
-10.67 MM-H20
724,69 MM-HG
37. C
16.8 IPS
.694 30-M
48042. SCNH
54167. ACMH
99.2
1.4
.201 NG/03CP
.01 KG/HR
.0 .•fl
f 9
701
71
;;:
MG. EPA 5

-------
cs
PMR
 TOTAL PARTICIPATE
 TOTAL PARTICULATE
   EMISSION RATE
   *  66
DE6 f,  29.92 IN.H6.

-------
                 EXAMPLE  PARTICIPATE CALCULATIONS TEST NO.  CDP-1

                                            OUT'
           VOLUME OF  DRV  CAS SAMPLED  AT  STANDARD CONDITIONS
           VM8TD •  (17.647 * VM * Y  *  (PB * PM / 13.6)) *  CTM * 460.)

  	.  _  _ .l7*»tt_*_Z68t68A *_1J.Q18 * _L.2(L.57_»  3.«»7._/.J3.6)___	__		   ..
           VM8TD •  ...........-...——...——————————.  •     249.509 DSCF
                                      (   98. * 460.)



  	VOLUME OF  MATER VAPOR *T  STANOARO,CONDITIONS	' , '. .	

           VMC » .04707  * VLC

  ••"•'•''•    VMC * ,»4TOf  *  ~t*» «" "":3'i*«"ttF;  ' ;  -\f'- "' "   '*  ' '' * ' ".   ' '; "~  " '''    P"   't  ;'  • " :-• W*W'r»i-v •-• *  ',     ~


»al
           PERCENT  MOISTURE IN STACK GAS

  T  '   "*'"" BUD • (tOO. * VWC) / (VM8TO « »MC)    '   f       ;:  ^ '":        •-:r~ ^ •  •  •  -V  ~~*     ^ <^^^^t,-T-, >. •-..---«, ..- '•  ^-


      P   §j,o' • ..."....liii.T.....;.".T..... «   U5T~PERCENT                '            ~                           "
      eL              249.509 *   3.84



  	MOLE^ FRACTION OF DR_T STA5JL-6M	'.	.	

           FMD • (100. • BNO) / 100.

  ' •> • '•'.            10t. -1.5   ~"   '  -:" ' '             T'  "'•    -''•"-     T~^"      ^    ^   *' !V    -*F"v-:-•••--TC   ;    -
           FMO « -*——.——.——•••« •   ,985



        *  AVERAGE  MOLECULAR NCItHT  OP ORt STACK 6AT    "^    r~^T   r^r—-    -j—    on	:	,-.,-, .-„,	 --^:



           MD > (   .00*44/100) •» (20.9*32/100) * ((79.1*  .0)  *  28/100 •   28.84



  	MOLECULAR  HEIGHT OF STACK_GAS					  _. 			_.	

"          MNS s MO * (1. - (BHO/100)) • 18. * (BHO/100)
f4	
"1^      :  MHS" ir~287»4* (1. -f l.51/100TF*TB. * 4 i.5l/tO«)  »  ' fa.67"       "   ~:~?  '     ?  '     :  a~~~l       "

-------
 STACK 6AS VELOCITY AT STACK CONDITIONS
 Otlf * lUlli OF THt iWTCVH • W* 4fO.J)
_V8_»_SS.49 *_Cf*_DELP./ _t»8RT(MM..jL.f8.>_-.            	.		
 VS • 89.49 •  .64 *  615.991 / (SQRT( 26.67 * 26.54)  •  26. •   55.23  FP9
                                                                                                                                   ^
.STACK 8AS JVOVUHETRIC rLONJ^
 09 • VS * AS * 3600/144"
as
                                     masts.
 STACK CAS VOLUMETRIC FLON AT STANDARD CONDITIONS
       *
 OSSTD
                                                   1.51/100))	
                    (  99. * 460.)
                                                                  1696562. 8CFH
 PERCfNT I9DKINETIC
 ISO • (305.58«CTS»4»0.))*((0.002»*9*VLC)»|VW*Y*(PB*(PM/13.6))/(TM*460.)))/(TT<»V9*P9*DN«DN)
                                                                               171
                                    251* *     53.23 *   26.54  *   .250  *   .250
VARTTCUCATl tOAOriWf*» EM OTTI
 C8 « O.OOi «_MN • l»««3 / VM8TQ
                                                                                                                                   -
 CS • 0.001 *     1.4 * 15.43 /   249.509
                                                .000  6R/08CF
_            LBSfMR ;__-•• _tf *__
 PMR • CS * OSSTO / (15.43 • 453.6)
 HI*
                                                      ToT
TTT*-
                                                                  'V- ,


-------
                                 APPENDIX A

                             EXAMPLE CALCULATIONS


 Yearly Emission Data Calculation for the Carter-Day Baghouse


 Average lead emis-  _  Process operating     Plant operation,     Mass emission
 sion rate, tons/yr     schedule, h/day           days/yr          rate, Ib/h

                     v 2000 Ib/ton

                     = (8) x (241) x (0.017) T (2000)

                     = 0.02 tons/yr


Production Rate Calculations for the Barton Oxide Process

Example - Run No.  2BOL-1
Amount of PbO                      /Sampling time \   Avg.  No.  of\
produced by each  = (2050 Ib/hog)  x/ _ (h)  _ \  x| hogs  charged]
process line                       1 Actual  operating)   1 during  first!
                                   \  time per shift/   \two shifts  /
                                   \    (h)       /
     PbO produced - (2050) x(|)x (12)  x (1.04)  -(2)  = 6400 Ib process  line

Production rate calculations for the past mixing operation

Example - Run No. ESL-2
                       \  sample run    /

                        (9.5) v (2.4) = 4.0 batches/h


                                    A-130

-------
Production rate calculation for the calcium lead alloy pasting operation

Example - Run No.  ESL - 3

     Number of     _/  Number of \  /Number of batches\  /Number of batches\
     plates pasted "plates pastedU  of paste mixed  Ix mixed during the  1
                    \  per shift /  \   per shift    /  \   sample run   /

                   = (80,910) T (7.5) x (3) = 32,364


     Equivalent number       / Number of   \ /Contingency^/Sampling \
     of batteries produced = yplates pastedy-^   factor  y  y time (h)y
     per hour
                           = (32,364) ~ (103) 4 (2.7) = 116 equivalent
                                                         batteries/h

     For processes  in which  the production rate is recorded by the plant,  the

following calculation was made to determine production rates during each

sample run.  For  these processes the actual operating time during a shift  is

the same.

     Process                N /Actual operating^ /camnl
    production    /Production), time during the  X(T. pl
    during each ~\  per shift/\   shift (h)    / Vt1me
    sample run


     Equivalent No. of   _/   Process      V/Contingency\ ^/Sampling
     batteries per  hour  "(production during]' \ factor  /'\time (h|
                           \each sample run/


Example - Run No. BIL-1
                        /        Total  \   /
     No. of plates     /       number of\  /      Actual   ,  ,     ,.   ,.   .
     parted at the   J,R ,?n   plates     . L  ., operating U, ?7 baijf'ln9
   automatic Machine ' 68'620  parted perfl7'33  time per ^3'27   time
        No. 1          V          shift   I  \      shift


                     = 30,581


     The same equation was used to determine the number of plates parted at auto-
matic No. 2 and manual machine.

     Equivalent No.   /Total No. of \  /Contingency^  /Sampling^
     of batteries   = Vplates parted/T V factor  /T\time  (h)/
       per hour                                  S   \      /
                    = (79,535) T (72) T (3.27) = 338 equivalent  batteries/h


                                     A-131

-------
     For processes in which the production rate is  recorded  by  the  plant  once

per hour the following calculation was made to determine  production rates

during each sample run.

                         /                 \  /
                         /Total production  \  /Sampling
     Process production _[    during hour    Uytime (h)
        rate per hour    1  sampled including!         '
                         ^fractions of hours/
                          \    tested     /



Example -  Run No. B2L-1


      No. of  batteries
      burned  at  the
      seven antimony     =  (168 +  57 + 132 + 164 + 151) T (2.8)
      lead  alloy MAC
      machines per hour

                        = 221  batteries burned/h
                                     132

-------
APPENDIX B




FIELD DATA
    B-l

-------
B-2

-------
                      TRAVERSE POINT LOCATION FOR CIRCULAR DUCTS
Plant
Date
Sampling location  £>p>- -fsn-'
Inside of far wall  to outside
 of nipple
Inside of near wall  to outside  of
 nipple (nipple length)     3.
Stack I.D.
Nearest upstream disturbance    ' ^—   dd
Nearest downstream disturbance   \ '•>.-' dd
Calculated by    ^ .•-•;	
                                                         >r
                                                         f-i
l-
                                                                   L-
                                                                  ~~
                                                            SCHEMATIC OF SAMPLING LOCATION
TRAVERSE
POINT
NUMBER
/

• ?
/ -/




















FRACTION
OF STACK I.D
<'. C'f: 7
.-"• • — s~"
r , / ^
('. ?7\




















STACK I.D
13. .s'
!






















FRODUCT OF
COLUMNS 2 AMD 3
(TO NEAREST 1 1 1NCH)
/
3 */e
/D /?
/a /?




















NIPPLE
LENGTH
^ 3~























TRAVERSE POINT LOCATION
FROM OUTSIDE OF NIPPLE
(SUM OF COLUMNS 4 t Si
•flte-^ v,
c ''A
' ? V^
"^^ /




















                                       B-3

-------
                                         CAS VELOCITY AND VOLUME DATA
1.
                PLANT AND CITY
/Qt*>A
                                                          RUN  DATE
                                                     J4     17
                                                                40
       SAMPLING  LOCATION
            CLOCK
            TIME
2.
RUN
NUMBER
v-s
OPERATOR
/-/tWASA'/'?-
AMB. TEMP.
CF)
. 9.V
BAR. PRESS
(in. Hg)
^T.5T5
STATIC PRESS
(in. H20)
- 0.Y
                                  21
MOLECULAR
WT.
..2.?. .
STACK INSIDE DIMENSION (in.)
3IAM OH SIDE 1
. /.1.S7 .
SIDE 2
i i • . .
PI TOT
TUBE Cp
o.n
MOISTURE
%
r * '
   40
               J«
                     FIELD DATA
TRAVERSE
POINT
NUMBER
7.8.9 ,10
*/£•/
XI
7
y
/V/£ '/
3-
3
H
/

































POSITION
(in.)
1 ,1 2 ,13 ( 14










































VELOCITY
HEAD
(Ap ) , in.H20
?5i26«J7I?B jj*
rt ."?f
o . yq
0 , A 2
r? , /5/f-
C>, 3 3
^> , V?

-------
                                    t cm
           ,N.|.|.|,|.|;M4,M..|.t|4.|	MMMi^litlitliniiNicl..!.,!..!
         ft/It Ei
                                             i i i  i i  i  i i i  i  i
                                                                     Mil
                                                     14Ul,ll,l,,|l,|40.|,,
                                                      1  1 > I  I i I—
                                                                                                   IOUIIW»
                                                                          ffi
                                                                                41 41 44|4S |4t 41 |4lU«|stkl SllSllvmS <
                                                                                                             I I I  I I
                                                                                                                               UHKI tm
                                                                                    H|t'|«M"l'»l"l"l"l"l'M"l"|"l>l|
                                                                                                                             KH i
           •« *>.
                                 OPtMIM
                    i»[«i<«i»iii|ii|it[I7I '''I
                                                                                       7"=r;o.oc-i  I
                                                                                                                MCIM
                                                                                                      _I_L
                                                                                                                      NUI UT
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                                                                                                                                             i   i

-------
                  LEAD SAMPLE RECOVERY AND INTEGRITY SHEET
                                            Sample date
r /
Sample location ^AUTOJLJ 0^.10^ gA&Haijser Recovery date
Run number^ 5?/)^ -/ Recovered by £Jj/
Filter number(s) Ofl,^ ,-J ,0 "7 7
MOISTURE
Impingers Silica gel
Final volume (wt) /£# ml (g) Final wt <2£S. 5 g
Initial volume (wt) ^^o ml (g) Initial wt 3cc>
Net volume (wt) ** /£ ml (g) Net wt /^S,^
Description of impinger water C^A?. /Oa

Total moisture ?o". A" g
g
g
% spent
Filter container number(s) 	
Description of particulate on filter
                              RECOVERED SAMPLE
                                            Sealed
Acetone probe
rinse container no.
Acetone blank
container no.
0.1 N HNOs probe
rinse container no.
Impinger contents
container no.
0.1 N HNOs blank
container no.
Samples stored and locked
Remarks
Liquid level
marked
Liquid level
marked
Liquid level
marked
Liquid level
marked
Liquid level
marked
                                                       X
                             LABORATORY CUSTODY
Received by
Remarks      "
                                                   Date
                                     B-6

-------
                                1M1 1 CM?
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-------
                  LEAD SAMPLE RECOVERY AND INTEGRITY SHEET
Plant
Sample location  t!a, 2-
Run number
                    -XI
Filter number(s)
Impingers
Final  volume (wt) _
Initial volume (wt)
Net volume (wt) 	
                               oxi*>£
                                            Sample date _
                                            Recovery date
                       000
Description of impinger water
                                      Recovered by  \|
 MOISTURE

_ml  (g)
_ml  (g)
_ml  (g)
                                             Silica gel
                                             Final wt
                                             Initial wt
                                             Net wt  2?, 7^2,0 = %£ 7
      . g
      . g
	g
 %  spent
                       Total moisture
                              RECOVERED SAMPLE
Filter container number(s)
                                            Sealed
Description of particulate on filter   H6-ftT
Acetone probe
rinse container no.
Acetone blank
container no.
0.1 N HNOs probe
rinse container no.
Impinger contents
container no.
0.1 N HNOs blank
container no.
                             ft
Samples stored and locked
Remarks
                                      Liquid level
                                      marked
                                      Liquid level
                                      marked
                                      Liquid level
                                      marked
                                      Liquid level
                                      marked
                                      Liquid level
                                      marked
                             LABORATORY CUSTODY
Received by
Remarks
                                                   Date
                                                             -/ 1  ~
                                    B-8

-------
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-------
                  LEAD SAMPLE RECOVERY AND INTEGRITY SHEET
Plant 	
Sample location
Run number
                   -3
Filter number(s)
Impingers
Final  volume (wt)
Initial  volume (wt)
Net volume (wt)
         C J?
                                            Sample date    ^/9/f/
                                                            I  I
                                            Recovery date    ••
                                      Recovered by
                                  MOISTURE
) 304
Wt) t2&£>
tJ
mpinger water
ml
ml
ml

(g)
(9)
(g)
Silica gel
Final wt
Initial wt
Net wt
^S-
Z44.fi g
0*50 g
y'^'. £> g
% spent
                       Total  moisture
Filter container number(s) _
Description of particulate on filter
                              RECOVERED SAMPLE
                                            Sealed
Acetone probe
rinse container no.
Acetone blank
container no.
0.1 N HNOs probe
rinse container no.
Impinger contents
container no.
0.1 N HNOs blank
container no.
                            /)
Samples stored and locked
Remarks
                                      Liquid  level
                                      marked
                                      Liquid  level
                                      marked
                                      Liquid  level
                                      marked
                                      Liquid  level
                                      marked
                                      Liquid  level
                                      marked
•f
-^
                             LABORATORY CUSTODY
Received by
Remarks
                                                   Date
                                    B-10

-------
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          /
-------
                PARTICULATE  SAMPLE  RECOVERY AND  INTEGRITY  SHEET
Plant 'pfgsT&i.jT'f
Sample location TiAKr&ju G%,i>~ gs^*
Run number cSBap-i
Sample date //9/fj
/ f
iausc Recovery date ''
Recovered by ^s^ff S^5s?
Filter number(s) &&O£ / 3O
Impingers ^ /&,
Final volume (wt) - c5 S u
Initial volume (wt) ^ic>a
Net volume (wt) ,j^ / ' &*-~~ft?~
Description of impinger water
MOISTURE
Silica gel
S ^"t1 wt "^^±^4
- 72^3— - c/, r n p n t

^?^t L
Total moisture
-JS3^^3~~^<3 g
Filter container nuniber(s)
                                RECOVERED  SAMPLE
                                              Sealed
Description of particulate on
Probe rinse
container no. ^~-9Aje kl an'<
container no. s~^
Liquid level
marked ^ e ^
Liquid level '
marked (^-^-^
Liquid level '
marked <-/ ^ ^>
I
Samples stored and locked ^t^-
Remarks

                               LABORATORY CUSTODY
Received by
Remarks     */
                                                  Date
                                      B-12

-------
                     TRAVERSE POINT LOCATION FOR CIRCULAR DUCTS
Plant

Date
Sampling location  J-
Inside of far wall  to  outside
 of nipple	
Inside of near wall  to outside of
 nipple (nipple length)    '	

Stack I.D.
T
Nearest upstream disturbance    '2.2.   dd

Nearest downstream  disturbance  "?. 5"   dd

Calculated by    y	
                                                           SCHEMATIC OF SAMPLING LOCATION
TRAVERSE
POINT
NUMBER
/
x,:
j">
"i
*;
(-
' 7
*
3.3 Vf
















NIPPLE
LENGTH
3 £T
I






















TRAVERSE POINT LOCATION
FROM OUTSIDE OF NIPPLE
(SUM OF COLUMNS 1 1 Si
V- '/j.
(p
* ,w
// :•'-'
-?r '/v
5 3 '/i
2?, CA
^7 '/a-
















                                       B-13

-------
                                           GAS VELOCITY AND VOLUME DATA
PLANT AND CITY
/h A *rc fi^^Tf^L , / C l*J A
i /
SAMPLING LOCATION
XrX 7~C i- & TT*/?.
CLOCK
TIME
0 1F°
RUN DATE
^16 J &\ $ /&\/
J4 17 40
2.
RUN
NUMBER
V-f
OPERATOR
P/3.Ctf*5/ , 
-------
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-------
LEAD
Plant Pz.t=-s7*t-/r^
Sample location _JJ^R£
Run number ££*. -/
Filter number(s) ^
Impingers
Final volume (wt)
Initial volume (wt)
Net volume (wt)
Description of impinger

SAMPLE RECOVERY AND INTEGRITY SHEET
Sample date &/?/&
s* f/uroLfT-ER. Recovery date
Kecovered by ^jr//
KXOaf?
MOISTURE
Silica gel
25--V ml (g) Final wt 4$,
A46 ml (g) Initial wt x/do
X4 0 ml (g) Net wt 
-------
                                                  EMISSION  TKSTiNo  MC.L.U  UMin
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-------
                  LEAD SAMPLE RECOVERY AND INTEGRITY SHEET
Plant *p7ie~sTz>ure Sample date ^Ifcti i ijji crir
Sample location ^x^a^cTse Sc^^uBK^e Recovery date *
Run number &£4.-<3 Recovered by vS"cr/V


Filter number(s) <3<3d^c5//
MOISTURE
Impingers Silica gel
Final volume (wt) lyy ml (q) Final wt 3-5
Initial volume (wt) ^^^ ml (q) Initial wt jc*
Net volume (wt) •yj ml (g) Net wt 33
Description of impinger water C^eA/e.

Total moisture 99. J 9
^. 7 g
i g
.? g
9^ % spent

Filter container number(s) 	

Description of particulate on filter
RECOVERED SAMPLE

     3        Sealed
Acetone probe
rinse container no.

Acetone blank
container no.

0.1 N HN03 probe
rinse container no.

Impinger contents
container no.

0.1 N HN03 blank
container no.
Samples stored and locked

Remarks
        Liquid level
        marked

        Liquid level
        marked

        Liquid level
        marked

        Liquid level
        marked

        Liquid level
        marked
                             LABORATORY CUSTODY
Received by
Remarks
                     Date
                                    B-18

-------
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                  LEAD SAMPLE RECOVERY AND INTEGRITY SHEET
Plant tter^Kx^r^ Sample date A/9/F/
Sample location X~x//b/ £TEJZ. Scjeuaxf* Recovery date
Run number fs^-J" Recovered by ^.JA/


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MOISTURE
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Final volume (wt) o2 73 ml (g) Final wt
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Remarks
                                                   Date
                                      B-21

-------
                                          EMISSION TESTING  FIELD  DATA
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-------
                PARTICULATE SAMPLE RECOVERY AND INTEGRITY SHEET
Plant
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                                                   Date
                                        B-23

-------
                        TRAVERSE POINT LOCATION FOR CIRCULAR DUCTS
Plant

Date
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-------
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-------
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-------

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-------
                  LEAD SAMPLE  RECOVERY AND  INTEGRITY SHEET
Plant "?£.e-iroLi r£ Sample date £//o/£-/
Sample location ZA&HAVS^ "*""? / Recovery date
Run number 4£Eej?> $12.-,^ Recovered by ^7/y


Filter number(s) ^ iT" «ool^S<
MOISTURE
u \^ ^ r ., . , .- ^ ^
Impingers Silica gel '
Final volume (wt) 38*^21 3 ml (g) Final wt
Initial volume (wt) <2£>c ml (g) Initial wt rjtf^
Net volume (wt) ^ i^ ml (g) Net wt o
Description of impinger water ^X£A£-

Total moisture /3 6 9
g
^ g
g
% spent

Filter container number(s)
RECOVERED SAMPLE
              Sealed
Description of particulate
Acetone probe
rinse container no. ^T-fT*
Acetone blank
container no. £"y
f
0.1 N HN03 probe
rinse container no. S^>
0.1 N HNOs blank
container no. J~V5
on filter \j&\tM /.AL. •

Liquid level x
^•V^? marked /
Liquid level
j5~; 4 marked '
Liquid level
IS /9 marked /
Liquid level
^X> marked f
Liquid level
3/) marked /
Samples stored and locked s^>'
Remarks

Received by U^yy^^^'
LABORATORY CUSTODY
v-+2^6~+ Date ^ ~ ' "7 -^ f
Remarks &

                                      B-31

-------
                                                 EMISSION  TESTING  FIELD  DATA
                               it MI t cm
                                               |l>|l>|H|ll|ju[M|n|«»|«
                                            i i I  I 1 I  M I  I I
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-------
                                              EMISSION  TESTING  FIELD  DATA
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-------
                  LEAD SAMPLE RECOVERY AND INTEGRITY SHEET
Plant   ftefsraLtrz	Sample date
Sample location 2?A6Ho,ise */	Recovery date
Run number  332 -j	Recovered by  ^
Filter number(s) 	
                                  MOISTURE
Impingers                                    Silica gel
Final volume (wt) 	Q_\^	ml (g)    Final wt 	3^6,,&	 g
Initial volume (wt)    303	ml (g)    Initial wt      £0^	 g
Net volume (wt) 	  / f	ml (g)    Net wt 	-y^. &	 g
Description of impinger water  dCe^R.       	%  spent
                       Total moisture
                              RECOVERED SAMPLE
Filter container number(s)    6~^~/^ Q	Sealed
Description of particulate on filter    1/rg.y (,
Acetone probe                         Liquid level
rinse container no.    T \/3A        marked
Acetone blank                         Liquid level
container no.          5 /5 y.^	  marked
0.1 N HN03 probe                      Liquid level
rinse container no.   T.'7JV)          marked
Impinger contents                     Liquid level
container no.         Tv/y/4          marked
0.1 N HNOs blank                      Liquid level
container no.         ,	Date
Remarks
                                       B-34

-------
                                           EMISSION  TESTING FIELD  DATA
                          fl/UI | (III
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-------
                                          EMISSION  TESTING  FIELD DATA

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-------
                PARTICULATE  SAMPLE RECOVERY AND  INTEGRITY SHEET
Plant p^esraurz:
Sample location fiAGrHfuts* * 1
Run number #3 ^~/
Filter number(s) £> £>c> 2 1 fe6
Impingers
Final volume (wt) ^to
Initial volume (wt) oito^
Net volume (wt) [o
Description of impinger water £ce

Total moisture
Sample date L/&/P/
/ *
Recovery date
Recovered by £j&

MOISTURE
Silica gel
ml(g) Final wt 3H&./
ml(g) Initial wt ^3tv\
ml (g) Net wt y f, /
A£- 'lO r- spent

5"?. / q



g
g
g

Filter container number(s)  	

Description of particulate  on filter
RECOVERED SAMPLE

              Sealed
Probe rinse
container no.
container no.
Impinger contents
container no.
        blank
container no.
Samples stored and locked

Remarks
   Liquid level
   marked

   Liquid level
   marked

   Liquid level
   marked

   Liquid level
   marked
Received by _

Remarks     &
                               LABORATORY CUSTODY
                  Date
                                      B-37

-------
                       TRAVERSE POINT LOCATION FOR CIRCULAR DUCTS
Plant
Date
                     /7£>
Sampling
Inside of  far wall to
 of nipple
                        >u,ts i de
Inside of  near wall to outside uj,,
 nipple  (nipple length) 	/•

                 <3^"
Stack I.D.
Nearest upstream disturbance    Q,
Nearest downstream disturbance _£rS
Calculated  by N  ; * $ '\r <
                                               f T
                                         dd
                                                                SCHEMATIC OF SAMPLING LOCATION
       TRAVERSE
         POINT
        NUMBER
                   FRACTION
                  OF STACK I.D.
STACK I.D.
   PRODUCT OF
  COLUMNS I AND 3
(TO NEAREST I/I INCH)
                           NIPPLE
                           LENGTH
TRAVERSE POINT LOCATION
FROM OUTSIDE OF NIPPLE
 (SM OF COLUMNS * I S)
                  0/6
           €
                  ,r?3f
           If
                                                                    33
           fe
                                      31V
                                                         V
                                              B-38

-------
                                        CAS  VELOCITY AND VOLUME  DATA
            PLANT AND  CITY
                                                          RUN DATE
                                                     0,4
                                                           J7     40
   SAMPLING LOCATION
                           CLOCK
                           TIME
                                     IK
RUN
NUMBER
£*V-/
OPERATOR
/^-v "• - J^
AKB. TEMP.
CF)
,7.5
BAR. PRESS
(in. Hg)
2.S.S.K
STATIC PRESS
(ir, . HjO)
- •
17 21 11 J5 )i
MOLECULAR
WT.
.^.°.
STACK INSIDE DIMENSION (in.)
31 AM OH SIDE 1
..-N r? . 7,«5,
SIDE 2
, . • . ,
PI TOT
TUBE Cp
•
MOISTURE
%
,/.*,
40 «« il ' •' •« »7 70 73 -H
                  FIELD DMA
TRAVERSE
 POIN'T
 NUV.DER
1-' ' ••> -'0
     ^
POSITION
  (in. )
           ^ .i? .i3«'
  VELOCITY
     HEAD
(ip
                            in.H-0
                     7 5.76 «7 7 . 78 ,7»
            •?<*•*/•*
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                          ' Z,
                          / .-r
  STACK.
TEKP, *F
                                    Je.39.40,4!
                                       9
                                                          4-
                                                             A
                                   B-39

-------
                    EMISSION  TESTING  FIELD  DATA
flMI 4 Clll
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-------
                                                      KMISSION  TESTING  FIELD  DATA
                                      4 cm
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-------
                  LEAD SAMPLE RECOVERY AND INTEGRITY SHEET
Plant PzesTs^/re- Sample date <&//////
> /
Sample location j?A£.nousr *<2 Recovery date
Run number s^l - / Recovered by &j/y
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MOISTURE
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rinse container no. 5~5/£ A
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                             LABORATORY CUSTODY
Received by            -            _ Date
Remarks     
-------
                                           EMISSION  TESTING FIELD  DATA
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-------
EMISSION TESTING FIELD DATA

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-------
                  LEAD  SAMPLE  RECOVERY AND INTEGRITY SHEET
Plant Pxe^TZ.L/rf
Sample location 3^**^* *
Run number S^A-^

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Sample date «J,A
Recovery date
„///

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Filter number(s) "5'?/x4
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level
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Remarks

                            LABORATORY CUSTODY
Received by _
Remarks     (/
                                                  Date
                                     B-45

-------
                                              EMISSION  TESTING FIELD  DATA
                                4 ciri
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-------
                                                       KMISSION  TESTING  FIELD DATA
                                       » on
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-------
                         LEAD SAMPLE RECOVERY AND  INTEGRITY SHEET
r 1 3 fl L f"^&s^&T&j j 7V-"
Sample location ^q/^^
Run number ££j_- f

MOISTURE
Silica gel
-2-Bo ml (g) Final wt £ -y.
3C& ml <(g) Initial wt ^oe
3?-" ml (g) Net wt 4
water /«£>«£>/•'

Total moisture 73-5" g
'3.-S g
->-
-------
EMISSION TESTING FIELD DATA

-------
                                                        EMISSION   TESTING   FIELD  DATA
                                     i  cm
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-------
                PARTICULATE SAMPLE RECOVERY AND INTEGRITY SHEET
Plant
Sample location  je/tey//iager
Run number   2J3P-/
                                              Sample date
                                              Recovery date
                                    Recovered by
Filter number(s)
                                    MOISTURE
Impingers
Final volume (wt) _
Initial volume (wt)
Net volume (wt)
                                           Silica gel
                                           Final wt
                                   ml(g)
        Initial  wt
        Net wt
                                                          43 .
Description of impinger water
                                                             spent
         f gy.
                    Total moisture
Filter container number(s) 	
Description of particulate on filter
                                RECOVERED SAMPLE
                                              Sealed
Probe rinse
container no.
container no.
 Impinger contents
 container no.
                       A
container no.
Samples stored and locked
Remarks
Liquid level
marked
Liquid level
marked
Liquid level
marked
Liquid level
marked
Received by
Remarks
                               LABORATORY CUSTODY
                                                   Date
                                    B-51

-------
                       TRAVERSE POINT LOCATION FOR CIRCULAR DUCTS
Plant
Date
Sampling  location	
Inside of far wall to  outside
 of nipple 	
Inside of  near wall  to  outside qf
 nipple  (nipple length)    /e, "
Stack I.D.       .
Nearest  upstream disturbance
Nearest  downstream disturbance
Calculated by
                                       Z, dd
                                      ^ dd
                                                                 SCHEMATIC OF SAMPLING LOCATION
        TRAVERSE
         POINT
        NUMBER
                   FRACTION
                  OF STACK 1.0.
STACK I.D.
   PRODUCT OF
  COLUMNS 2 AND I
(TO NEAREST 1 \ INCH)
                           NIPPLE
                           LENGTH
TRAVERSE POINT LOCATION
FRO* OUTSIDE OF NIPPLE
 (SUM OF COLUMNS 4 t 5)
           3
                                         3 »ft -
                                          5/z"
                                                                       *W
           /o
                                               Xa"

                                           B-52

-------
                                          CAS VELOCITY AND VOLUME  DATA
PLANT AND CITY

1
SAMPLING LOCATION
/&*3 &<,((,
CLOCK
TIME

RUN DATE
-,£LJ. \..,J.-'\.
}4 )' *0
1.
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OPERATOR
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                                              STATIC PRESS
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    t',i 1' ' 1
                                              11
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TUBE Cp
•
MOISTURE
%
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40 '« J« •' •' *7 70 73 It
                     FIELD DMA
     TRAVERSE
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(ip ) ,  in .HO
  STACK
TEMP,  *F
                        ?5,76«J7, 58 ,J*::6, 39.40, 11
                2 7
                                *:   -^.^?"^,&
                                                           '-   if I
                                 B-53

-------
                                                       EMISSION TESTING FIELD DATA
                                         t cm
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-------
                  LEAD SAMPLE RECOVERY AND INTEGRITY SHEET
Plant p£.csfa±/rf Sample date 4/<9jP/
Sample location fiA^p^iz? *3 Recovery date ^fa/fr
Run number $3± -/ Recovered by  g
J?>CL> g
z
-------
                                                      EMISSION TESTING  FIELD  DATA
                                  flMt * Clff
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-------
                  LEAD SAMPLE RECOVERY AND INTEGRITY SHEET
Plant  pf£sjoL/T€:	Sample date
Sample location   J^v."0 I 3 7	   	
                                  MOISTURE
Impingers
Final volume (wt)
Initial volume (wt)
Net volume (wt)
Description of impinger
/9r mi
<200 ml
-.< ml
water (* r &z
(g)
(g)
(g)
K-
Silica gel
Final wt 2$"?,
Initial wt .303
Net wt .s~9, /
//•^
/ 9
g
g
% spent
                       Total  moisture
                              RECOVERED SAMPLE
Filter container number(s)   *f<,«yj g	Sealed
Description of particulate on
Acetone probe ^sY^f
rinse container no. - tfyftyv
Acetone blank
container no. &J&/A
0.1 N HNOs probe ^St&A
v* i n «; A rnntrHnnr nn _-*4^<3 ^/ ^

Impinger contents
container no. .^"-y^oV?
0.1 N HNOs blank
container no. &V33fl
filter l-j(rfiT GH.AI

* Liquid level
9 marked /
Liquid level
marked /
Liquid level
marked ^
Liquid level
marked /
Liquid level
marked /
Samples stored and locked x*^z_
Remarks (/

Received by Q#r*Jl>*, ^^
LABORATORY CUSTODY
. +-E-LA-.'*, nx /a — 7 "7 .— 0 /
*^^&*^ Date ^ / / V (
Remarks L/

                                      B-58

-------
cffi
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   I
   4!

                                B-59

-------
                                                          EMISSION  TESTING FIELD  DATA
                                            Cllf
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-------
                  LEAD  SAMPLE  RECOVERY AND  INTEGRITY SHEET
Plant 'Pzff.Tcur^ Sample date fr/ta/G-/
i 7
Sample location £/q^Na^,- ** 3 Recovery date
Run number B3I-3 Recovered by ,- ^S/A
0.1 N HNOa probe
rinse container no. 5T/d/^
Impinger contents
container no. ^.T^/./?
0.1 N HN03 blank
container no. 5'/£'3A
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marked /
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Remarks

LABORATOI
/I J-
Received by C^'0^*^. •i'Ts-+«'*o*-
RY CUSTODY
Date £^f 7- ^/
Remarks C/

                                     B-61

-------
                                                      EMISSION  TESTING  FIELD  DATA
                                      4 cm
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-------
                                                           EMISSION  TESTING  FIELD  DATA
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-------
LEAD SAMPLE  RECOVERY AND  INTEGRITY SHEET
Plant &3tS7BL/re Sample date £*/"/&
Sample location KA&HOUS*? *^ Recovery date
• /
Run number g-^z-y Recovered by <$JH
Filter number(s) <^CO33.3'2
MOISTURE
Impingers Silica gel
Final volume (wt) 303 ml (g) Final wt
Initial volume (wt) ^oo ml (q) Initial wt
Net volume (wt) 3 ml (q) Net wt
Description of impinger water (^L^A^

Total moisture 
-------
                                                       EMISSION  TESTING  FIELD  DATA
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-------
                                                     KMISSION  TESTING  FIELD  DATA
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-------
               PARTICULATE SAMPLE RECOVERY AND INTEGRITY SHEET
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Recovery date
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-------
                     TRAVERSE POINT LOCATION FOR CIRCULAR DUCTS
Plant
Date
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-------
                                       CAS VELOCITY  AND VOLUME DATA
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-------

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-------
                  LEAD SAMPLE RECOVERY AND INTEGRITY SHEET
Plant Pxe<>rat,r£ Sample date /i/f/f/
Sample location ^^^T^e-Z^v EAA-HC^S,- Recovery date
Run number CDA~/ Recovered by grrtj
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rinse container no.  £~-y3
-------
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-------
                  LEAD SAMPLE RECOVERY AND INTEGRITY SHEET
Plant ^ZC^JOC/TS^ Sample date <;>'»; 'jy
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f
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container no.

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                             LABORATORY CUSTODY
         by
                     Date
Remarks
                                    B-75

-------
                                              EMISSION  TESTING  FIELD  »ATA
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-------
                                                 EMISSION  TESTING  FIELD  DATA
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-------
                  LEAD SAMPLE RECOVERY AND INTEGRITY SHEET
Plant pj^e^r^Ljr^ Sample date *.
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                             LABORATORY CUSTODY
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Remarks
                                                   Date
                                       B-78

-------

-------
                                                    EMISSION  TESTING  FIELD  DATA
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• i

-------
                PARTICULATE SAMPLE RECOVERY AND INTEGRITY SHEET
Plant
Sample location
Run number
                             /?A£.M/,US^-
                                              Sample date
                                              Recovery date
                 - 1
                                    Recovered by
Filter number(s)
                            s
                                    MOISTURE
Impingers

Final  volume (wt)

Initial  volume (wt)

Net volume (wt)
.) _}J25
Wt) «Jfc)£)
£ < ^
mpinger water £
ml(g)
ml(g)
ml(g)
L&AA.
Silica gel
Final wt
Initial wt
Net wt

&0 5^ - S-
^>0o
S£ ^
/<3tf - spent
9
9
9

                    Total moisture
                                         P7.
Filter container number(s) 	  	

Description of particulate on filter
                                RECOVERED SAMPLE

                                              Sealed
Probe rinse
container no.

       <=-b1ank
container no.
Impinger contents
container no.
 >Etft   blank
container nr.
Samples stored and locked
Remarks
                                   Liquid level
                                   marked

                                   Liquid level
                                   marked

                                   Liquid level
                                   marked

                                   Liquid level
                                   marked
                                                    x
Received by
Remarks
                               LABORATORY  CUSTODY
                                                   Date
                                                            - /
                                      B-81

-------

-------
    APPENDIX C




LABORATORY RESULTS
       C-l

-------
C-2

-------
                                PEDCO ENVIRONMENTAL, INC.
                      LABORATORY DATA
                                                   1 1499 CHESTER ROAD
                                                  CINCINNATI, OHIO 45246
                                                        (513) 782-47OO
                                               TELECOPIER (513) 782-48O7
Run No.

B1L-1
B1L-2
B1L-3
B2L-1
B2L-2
B2L-3
B3L-1
B3L-2
B3L-3
B3L-4
ESL-1
ESL-2
ESL-3
BOL-1
BOL-2
BOL-3
CDL-1
CDL-2
CDL-3
        Lab Numbers
BX152,
BX153,
BX154,
*BX155,
*BX156,
*BX157,
BX158,
BX159,
BX160,
BX161,
BX162,
BX163,
BX164,
*BX165,
*BX166,
*BX167,
BX168,
BX169,
BX170,
171,
172,
173,
174,
175,
176,
177,
178,
179,
180,
181,
182,
183,
184,
185,
186,
187,
188,
189,
190,
191,
192,
193,
194,
195,
196,
197,
198,
199,
200,
201,
202,
203,
204,
205,
206,
207,
208,
209
210
211
212
213
214
215
216
217
218
219
220
221
222
223
224
225
226
227
                         Net mg,
                           Pb

                          11.1
                          8.23
                          7.34
                          2.37
                          2.66
                          2.68
                          2.18
                          3.23
                          5.33
                          4.67
                                      2,
                                      5,
                            48
                            43
                          4. 30
                          31.7
                          47.3
                          74.0
                          1.30
                          0.98
                          0.90
                 * Value obtained by method of  additions
                      Audit Filters
 Number

832-3592
832-8573
832-9700
Lab. No.

 BX323
 BX324
 BX325
True Value

  0.800
  2.00
  2.40
mg. Pb

 0.782
 2.06
 2.40
Recovery

 97.8
 103
 100
                               BRANCH OFFICES
                               03
 CHESTER TOWERS
                       DALLAS, TEXAS

                    KANSAS CITY, MISSOURI
                          COLUMBUS, OHIO

                       DURHAM, NORTH CAROLINA

-------
                                PEDCO ENVIRONMENTAL, INC.
                      LABORATORY  REPORT
                                                    1 1499 CHESTER ROAD
                                                   CINCINNATI, OHIO 45246
                                                         (513) 782-47OO
                                                    TELEX (513) 782-48O7
Run  No.

BOP-1

B2P-1

CDP-1
Front Half
   17.9
   3.12
   1.42
Lead, mg

Back Half
    *

   0.14

   0.02
Total

17.9

3.26

1.44
* not requested
                                BRANCH OFFICES
CHESTER TOWERS
                      DALLAS. TEXAS
                    KANSAS CITY, MISSOURI
                           COLUMBUS, OHIO
                        DURHAM, NORTH CAROLINA
                               C-4

-------
               BLANK  ANALYTICAL DATA FORM
plant
                       P//NJ
                 Uh  **•  BX i3 I
Sample location
Relative humidity
Liquid level marked  and  container sealed

Density of acetone  (pa)

Blank volume  (Va)
                                                             g/ml •'

                                                              rruU
Date and time of wt  6-9-3--8 I   8'*O&a^ Gross wt	

Date and time of wt  ^>'9~^'8l   ^"15 o*\ Gross wt   \O'p3^OQ.ci mg
                                Average  gross wt

                                         Tare wt

                           Weight  of  blank (ma)
                                                    IO53-O8.& mg "

                                                        ^l-^- mg -
                                                        17.4-  mg •/
                        m.
                      va  Pa
                                                       .D35 mg/g
                                    )
Note:  In no case should  a  blank  residue greater than 0.01 mg/g)
or 0.001% of the blank weight  be  subtracted from the sample
wei(?ht-
Filters
Date and time of wt
Date and time of wt  <
-------
                   BLANK ANALYTICAL DATA
Plant   U.6.
                                                        /33
Sample location
                                                     545.3- fl
Relative humidity

Type of blank 	
Liquid level at mark and container sealed 	

Density of blank  (pa)    I>O	 g/ml

Blank volume (Va)
                                              yes
Date and time of wt.

Date and time of wt.
                           - $t
ml y

Gross wt.  /Q.,1736-7 mg "

Gross wt.  /Q273fc-3 mg"
                                 Average  gross wt.  /Q3L73fc.Smg

                                           Tare wt.  103-728. j> mg ^

                              Weight of blank  (ma)      8.3. mg ''
          Ca =
                 ma
               Va pa
                               (  t.O  )
                                      =   -O/7
         mg/g
Note:  In no case shall a blank  residue  greater than (0.01
mg/g) or 0.001% of the weight of blank used be subtracted
from the sample weight.
Remarks:
                         in
          Signature of  analyst

          Signature of  reviewer
                              C-6

-------
                   BLANK ANALYTICAL DATA
Plant
         U.6.   LPf\
Sample location
Relative humidity

Type of blank
                        -  h log
                               o
Liquid level at mark and container sealed 	

Density of blank (pa)    /.P^/g	 g/ml

Blank volume (Va)
                     I5D

Date and time of wt.  6-^-8 <  B'-OO

Date and time of wt.  6
                                         ml"

                                         Gross wt.

                                         Gross wt.
                                 Average gross wt.

                                          Tare wt.

                              Weight of blank  (ma)
          r_
          Ca
                 ma
                                                           nig-
                                                          .*f mg

                                                          6 mg
                                                         .& mg -
Note:  In no case shall a blank residue greater  than  (0.01
mg/g) or 0.001% of the weight of blank used be subtracted
from the sample weight.
Remarks:
           . Ol
                        to
          Signature of analyst

          Signature of reviewer
                                              15
                                     •s       .
                                     £C-L(-   O- AO tx-
                               C-7

-------
         METHOD 5 TRAIN ANALYTICAL PARTICULATE  DATA
Plant  U.5. Lf>R
                                               Run  No.
Sample location 	
Relative humidity 	
Density of acetone  (pa)
                                                      g/ml
Sample
type
Acetone rinse
filter (s)
Sample
identifiable
Ve6
ye-a
Liquid level at mark
and/or container sealed
V^S
yd*S
Acetone rinse container no.
Acetone rinse volume  (Vaw)
                                                   ml"
Acetone blank residue concentration  (Ca)  .Ol
Wa = Ca Vaw pa =  ( .O\ ) ( /g,) =   /»5
Date and time of wt Jh_~/7~8l 3-
Date and time of wt  (c
                              8:0D
                                       Gross wt
                                       Gross wt
                                                         mg/g '
                                                         mg >
                                                         S mg"
                                                        .D
                               Average gross wt
                                        Tare wt
                     Less acetone blank wt  (Wa)
         Weight of particulate in acetone rinse
Filter (s) container no.  BX /66 *0oo3-?-l~} ($<4bS6)
Date and time of wt  &~/~? -j
Date and time of wt  (0-17-$
                                                           mg
                                                  6>6>8£34--3 mg
                                                       /^S  mg
                                                     37.Q mg
                              5 '
                                        Gross  wt
                                        Gross  wt
                                                           mg
                               Average  gross  wt
                                         Tare  wt
             Weight of particulate  on filter (s)
         Weight of particulate in acetone  rinse
                    Total weight of particulate
                                                           mgt
                                                     76 -S  mg./
                                                      37.0  mg
                                                    //3-5  mg ^
Note: In no case shall a blank residue  greater than (.01 mg/g) or
.001% of the weight of acetone used  be  subtracted from the sample
weight.
Remarks:

Signature of analyst (
Signature of reviewer
^U/bt^ (WcS
' J t --A- /Oc /w C/--T-C

rJ /V.
                               C-8

-------
         METHOD 5 TRAIN ANALYTICAL PARTICULATE DATA
Plant   U.S. CPA
                                              Run No.
Sample location 	
Relative humidity   5oc/c
Density of acetone  (pa)
                                                     g/ml
Sample
type
Acetone rinse
filter (s)
Sample
identifiable
yes
yeS
Liquid level at mark
and/or container sealed
\?d5
V£5
Acetone rinse container no.  E>K /85
Acetone rinse volume  (Vaw)
                                                  ml
Acetone blank residue concentration  (Ca)
Wa = Ca Vaw pa =  ( - & I ) (
                                          .Ol
Date and time of wt
Date and time of wt
                     &-/3-&I
                                       Gross wt
                                       Gross wt
                                                        mg/g*
                                                        mg -S
                                                       • O mg'-
                               Average gross wt
                                        Tare wt
                     Less acetone blank wt  (Wa)
         Weight of particulate in acetone rinse
Filter(s) container no.
Date and time of wt   (o
Date and time of wt
                                                 77*f3-£>. ^- mg "
                                                       > -P- mg •
                                                 7738O-8
                                                      2-d- mg i-
                                                     *43-3i. mg -
                     6-/7-8/
                                       Gross wt
                                       Gross wt
                                                   37 7.
                                                          mg-
                                                    37 7- g mg-
                               Average gross wt
                                        Tare wt
             Weight of particulate on filter (s)
         Weight of particulate in acetone rinse
                    Total weight of particulate
                                                    377.
                                                          ing-
                                                          mg
                                                      7Q-O mg
Note: In no case shall a blank residue greater than  (.01 mg/g)  or
.001% of the weight of acetone used be subtracted  from  the  sample
weight.
Remarks:
     Signature of analyst
     Signature of reviewer
                                C-9

-------
Plant
         METHOD 5 TRAIN ANALYTICAL PARTICULATE  DATA
                                              Run No.
Sample location 	
Relative humidity  SOc/c
Density of acetone  (pa)
                                                      g/ml
Sample
type
Acetone rinse
filter (s)
Sample
identifiable
y«?5
yes
Liquid level at mark
and/or container sealed
VtS
yes
Acetone rinse container no.
Acetone rinse volume  (Vaw)
                                                  ml
Acetone blank residue concentration  (Ca)
Wa = Ca Vaw pa =  ( ,C I  ) ( 2>fl3 •s'
Date and time of wt 6-/?-£?/ ^j.'i^a^     Gross wt
Date and time of wt &'/? ~Q \  3-'3Op^->   Gross wt
                               Average gross wt
                                        Tare wt
             Weight of particulate  on filter (s)
         Weight of particulate in acetone rinse
                    Total weight of particulate
                                                  635g^-q mg^
                                                  k?3S53-O mg -
                                                 	I'B  rog -
                                                           mg'
                                                           mg "
                                                        4?  mg
                                                           mg •'
                                                           mg •'
Note: In no case shall a blank  residue  greater than (.01 mg/g) or
.001% of the weight of acetone  used  be  subtracted from the sample
weight.
Remarks:
     Signature of analyst
     Signature of reviewer
                                ^
                                                       •r.i-N.
                             c-io

-------
                                                        Page 1 of 2
             Analytical Organic Particulate  Data
Plant
                      35^5 -/7
Run No.
Sample location.
Relative humidity  5O°/c
Density of acetone  (pa
                                                        g/ml
Sample
type
Acetone rinse
Impinger rinse
Filter (s)
Sample
identifiable
^S
y^S
y-e-S
Liquid level at mark
and/or container sealed
V ~^-$
yo
^
FRONT HALF
Acetone wash of nozzle, probe, cyclone
 (bypass), flask, front half of filter           \
 holder.      Container no.   BX  /43    CSV-?? A)
Date and
Date and
Filter (s
Date and
Date and
time of wt. (e'3-3-~'$t i-OO^--^, iross wt. i
time of wt .  L -7«*8J - 2-8., Average gross wt.
Tare wt.
Less acetone blank wt. (Wa)
Weight of particulate in acetone rinse
) container no. £'X IV7 **- ooa P-/3O (_ *=><+?
time of wt. (e>~l~l~&( *4>?>Op^ Gross wt.
time of wt. (e~(1-tfl ^.$o
-------
                                                         Paqe 2 of  2
BACK HALF ETHER- CHLOROFORM EXTRACTION

Impinger contents  and  water wash of
 impingers, connectors,  and back
 half of filter holder.   Container no. OX
                                                           ,.
                                                   L 5*4-?" 4)
Inorganic fraction container no.  oX
Date and time of wt.

Date and time of wt.
                               ?'3> £><>->•» Gross wt.
         —     , C ' ' ^J ~ ^T • O  ./'
                                 Average gross wt.

                                          Tare wt.

                              Less water blank wt.

                 Total  weight of inorganic phase

Organic fraction container  no.__cX_

Date and time  of wt.  fc?~P*3-'a/  y-OCxz-^  Gross wt.
Date and time of wt.

   (-01} (-  /5C)  (
                                         Gross wt.
                        ''k '     Average gross wt._

                                          Tare wt..

                   Less  ether-chloroform blank wt..

                    Total  weight of organic phase _

                               BACK HALF SUBTOTAL .

                                     TOTAL WEIGHT
                             f t I   .//
     Signature of  analyst 	
     Signature of reviewer.
                                         Gross wt.    /£)7333 7-6
                                                       /£7533-4
                                                             f.5
                                                             I."?
                                                               -t
                                                             7-7
                                                                   mg-
 mg'-

. mg4-

. mg v

/

 mg "

. mg -



. mg"

.mg-''

 mg "

 mg^

 mg "
                            C-12

-------
         METHOD  5 TRAIN ANALYTICAL PARTICULATE DATA
Plant
                     35^-5-77
                        Run No.
Sample location 	
Relative humidity
Density of acetone  (pa)
                                                      g/ml
Sample
type
Acetone rinse
filter(s)
Sample
identifiable
l/«?-S
yn
Liquid level at mark
and/or container sealed
V£5
y^s
Acetone rinse container no.
Acetone rinse volume  (Vaw)
                             EX. 181   5*^3- A
                                                   ml
Acetone blank residue concentration
Wa = Ca Vaw pa =  (.O \   ) ( P-^-?  ) (:
Date and time of wt  (s
Date and time of wt  £
              (Ca)
               )  =
                                           .01
                                          P--3
                                        Gross wt
                                        Gross wt
                                                         mg/g ''
                                                         mg ^
                                                         7  mg -
                               Average gross wt
                                        Tare wt
                     Less acetone blank wt  (Wa)
         Weight of particulate in acetone rinse
Filter (s) container no. gX lb3L*ooo33$3 ($>44,3-a^,
Date and time of wt  £-/7-gj  ^'/5<^»   Gross wt
Date and time of wt
                           (o(cSoS-Q  mg
                                    mg'
                                    mg>
                                    mg<
-/ ?'<;>./. ^_' Bo
                                       Gross wt
                                                    355.0
                               Average  gross  wt
                                         Tare  wt
             Weight of particulate  on filter (s)
         VJeight of particulate in acetone  rinse
                    Total weight of particulate
                                                    3t> i -to
                                                      33
                                                      ID.
mg/

mg •
mg •
mg -
                                    mg
                                    mg
Note: In no case shall a blank residue  greater than (.01 mg/g) or
.001% of the weight of acetone used  be  subtracted from the sample
weight.
Remarks:
     Signature of analyst
     Signature of reviewer
                               C-13

-------
         METHOD 5 TRAIN ANALYTICAL PARTICULATE DATA
Plant  U.S.
                   35^-5 -
                                              Run No.
Sample location
Relative humidity   50
Density of acetone  (pa)  - 7^0 &
                                                      g/ml
Sample
type
Acetone rinse
filter (s)
Sample
identifiable
yes
yes
Liquid level at mark
and/or container sealed
y^5
y^s
Acetone rinse container no.
Acetone rinse volume  (Vaw)
                             B X.
                                       54-7 / 4
                                                  ml
Acetone blank residue concentration  (Ca)
Wa = Ca Vaw pa =  ( .Ol ) ( sof  ) ( D^oQ) =
                                           ,O(
Date and time of wt
Date and time of wt
                                       Gross wt
                               8.'ooX. /6S **c>ooAP^/ ($4-7 < <3) ^
Date and time of wt  &-/7-&I  tf.'/Sa™   Gross wt
Date and time of wt  &'/8'B(  9>',?>Oa^ Gross wt
mg/g '
mg '

-------
         METHOD 5 TRAIN ANALYTICAL PARTICULATE  DATA
          > -5.
Plant 	
Sample location 	
Relative humidity  f>O c/0
                                              Run No.
Density of acetone  (pa)
                                                      g/ml
Sample
type
Acetone rinse
filter (s)
Sample
identifiable
/£S
yes
Liquid level at mark
and/or container sealed
V£5
y^S
Acetone rinse container no.  BX. / 83
Acetone rinse volume  (Vaw)
                                                   ml -
Acetone blank residue concentration
Wa = Ca Vaw pa =  ( .Ct  ) ( ;uf&  )
Date and time of wt _6~/*?-8/   «
Date and time of wt  (o
                                     (Ca)   .Of
                                                        mg/g.
                                       Gross wt  (obbi /•$  mg"
                                       Gross wt  (y(g3/ 8 • Q  mg •'
                               Average gross wt
                                        Tare wt
                     Less acetone blank wt  (Wa)
         Weight of particulate in acetone rinse
Filter(s) container no. BX
Date and time of wt  (&~n-\
Date and time of wt
                                                  fefe3<7.8  mg
                                                  fc»63f /• O  mg
                                                 	/.*?  mg
                     £?'/7-8<
                                       Gross wt
                                       Gross wt
                                                   363 -
                               Average  gross wt
                                        Tare wt
             Weight of particulate on filter (s)
         Weight of particulate in acetone  rinse
                    Total weight of particulate
       mg^

       mg "
       mg -
	 mg '
 3
-------
                                                        Page 1 of 2
             Analytical Organic Particulate Data
Plant
             . LPft
                                              Run  No.
Sample location.
Relative humidity _

Density of acetone  (pa)  • ' X 138 M OOO 3~3-V% £64-?
time of wt. <£>'/?-?/ lo'.boc.-^ Gross wt.
time of wt. fo"/7'8/ I7'3C'<^-^ Gross wt.
Average gross wt.
Tare wt.
Weight of particulate on filter (s)
Weight of particulate in acetone rinse
Total weight of particulate
FRONT HALF SUBTOTAL
C-16
O^^l 3~*~> O
^o ' if- <-> ••— mg1'
(£>3£1 5-^f"-~? mg*-
IO£c13.q-;Q mgi
/c?3t?o4--9 mg»
/>'<-? mg ^
< ^r q
1 ->• i mg "'
fafi^ ^
«3<^>£7 • / mg u
36 5. ^ mq^'
**S t^ ^^ . S< y'
**j ^*~ *~^ fi mo ^
350.3 mg-
/5-S ing i/
/
/ ^7 *•?
Ol-^r mg "
OI-*-r mg^
f.;*-'O)
                                                                     •*l.

-------
                                                         Page 2 of  2
BACK HALF ETHER-CHLOROFORM EXTRACTION



Impinger contents  and  water wash of

 impingers, connectors,  and back        _

 half of filter  holder.   Container no.  PA
     Signature of reviewer
Inorganic fraction  container no. D>C /oO  '4-ty "	f~>Oo ,



Date and time of wt.  6"/?'8/  ^C? M 5 • S   mg
Date and time of wt.   ^'<^^'3>  O'3o g-^ Gross wt.	fc^fe* i \^>-<->   mg



     /.CO ( '3oj ( /f
-------
         METHOD 5 TRAIN ANALYTICAL PARTICULATE DATA
Plant   Ci.5. LPA
                                              Run No.
Sample location 	
Relative humidity
Density of acetone  (pa)
                                                     g/ml
Sample
type
Acetone rinse
filter (s)
Sample
identifiable
ttf>
VeS
Liquid level at mark
and/or container sealed
yet>
\/£S
Acetone rinse container no.
Acetone rinse volume  (Vaw)
                                171   5601
                                                  ml
Acetone blank residue concentration  (Ca)
Wa = Ca Vaw pa =  ( .Ol ) ( +(cb ) (.7a^  Gross wt  _
Date and time of wt  k-ll'%1  3-"-30^,^   Gross wt
                                                    3^7-5 mg
                    	'jA»>
                               Average gross wt
                                        Tare wt
             Weight of particulate on filter(s)
         Weight of particulate in acetone rinse
                    Total weight of particulate
                                                           mg
                                                           mg
Note: In no case shall a blank residue greater  than  (.01  mg/g)  or
.001% of the weight of acetone used be subtracted  from the sample
weight.
Remarks:
     Signature of analyst
     Signature of reviewer
                                 C-18

-------
         METHOD 5 TRAIN ANALYTICAL PARTICULATE DATA
Plant
                         35P-5-/7
                                               Run No.
Sample location 	
Relative humidity 	
Density of acetone  (pa)
                                                      g/ml
Sample
type
Acetone rinse
filter (s)
Sample
identifiable
v/eS
vfd-'S
Liquid level at mark
and/or container sealed
ves
Ve-S
Acetone rinse container no.
Acetone rinse volume  (Vaw)
                                           550 ^
                                                   v
                                                   ml
                                           . O t
Acetone blank residue concentration (Ca)  	
Wa = Ca Vaw pa =  ( , O (  ) ( 3^3  ) ( -~7O<9-w.  Gross wt
                                Average gross wt
                                                         mg/g •/
                                                         mg -
                                                           mg -
                                                           mg '
                                                           mg "
                                         Tare wt  6^34-0 mg
                                                      3. i  nig
                                                      IP- Q mg
                                                    	mg
                                                     36/- /  mg
                                                         2 mg
                     Less  acetone blank wt (Wa)
         Weight of particulate  in acetone rinse
Filter(s) container no. 5X./53 ** ODD tf?5 (5So4-d]
Date and time of wt  (o'l~7-^\  tf'.iSa™    Gross wt
Date and time of wt  ^-/7'P/  3-3Ox?,-n    Gross wt
                                Average gross wt
                                         Tare wt
             Weight of particulate on  filter(s)
         Weight of particulate  in acetone rinse
                    Total  weight  of particulate
Note: In no case shall a blank  residue greater than  (.01 mg/g) or
.001% of the weight of acetone  used be subtracted from the sample
weight.
Remarks:
                                                     567-Q n»g
                                                       ^/.O mg
                                                           mg
                                                           mg
                                                      IO.Q
     Signature of analyst
     Signature of reviewer
                                                       .--  n
                                                       1 • J -IV
                               C-19

-------
         METHOD 5 TRAIN ANALYTICAL PARTICULATE DATA
Plant  #.6.
                                              Run No.
Sample location
Relative humidity  5<3
Density of acetone  (pa)
                                                     g/ml
Sample
type
Acetone rinse
filter(s)
Sample
identifiable
V£S
V<^S
Liquid level at mark
and/or container sealed
yes
V<£S
Acetone rinse container no.
Acetone rinse volume  (Vaw)
                             5X O3
                                                  ml'
Acetone blank residue concentration  (Ca)
Wa = Ca Vaw pa =  (,oi
                                           .01
Date and time of wt
Date and time of wt
                                       Gross wt
                                       Gross wt
                                                        mg/g•
                                                        mg  '
                                                        
-------
                                                        Page 1 of 2
             Analytical Organic Particulate  Data
Plant   a-**  tPf\    3536-17
Run No .
           i r  I
Sample location
Relative humidity
Density of acetone  (pa
          g/ml
Sample
type
Acetone rinse
Impinger rinse
Filter (s)
Sample
identifiable
yes
yes
^es
Liquid level at
and/or container
mark
sealed
NJC5
y&s
^£S
FRONT HALF

Acetone wash of nozzle, probe, cyclone
 (bypass), flask, front half of filter         N
 holder.      Container no.  BK / 4O   C SSO"? A)
Date and
Date and
Filter (s)
Date and
Date and
time of wt. (o"l^~Bl ^'-OO^.^
time of wt. ( CWOB): 3.5, Average
Less acetone blank
Weight of particulate in acet
container no. £>X IS4/- *^ Ctoo,2
time of wt. £?~/?~cJ' /C-SO^-^
time of wt. fe-/*7"8< ^/'•'3o^'>-»
r
Average
Weight of particulate on
iross wt. /^3SO. I ma^
Gross wt. 10*^3 7<-?-'~7 mg1^
gross wt. /0Af376t,S mg-x
gross wt. 3fc6.^^^^X
' 7^;/'.

-------
                                                         Paqe 2 of 2
BACK HALF ETHER-CHLOROFORM  EXTRACTION

Impinger contents and water wash of
 impingers, connectors,  and back
 half of filter holder.   Container no.

Inorganic fraction container no.   OX

Date and time of wt.

Date and time of wt.
        ¥50) £/..
                                    Gross wt.
                                ?-'5o «a-~->  Gross wt.
Date and time of wt._±
 (..01}  C/5o) (.1.019)--  /.fe
                                    Gross wt.
                           Average gross wt..

                                     Tare wt..

             Less ether-chloroform blank wt..

              Total weight of  organic phase

                          BACK  HALF SUBTOTAL .

                                TOTAL WEIGHT .
                       /? ;    . D
Signature of analyst .
                                                            /•€>
                                          Tare wt.     IC>?5~~}S-£.

                              Less water blank wt.	• 'S

                 Total weight of inorganic phase 	'' /

Organic fraction container  no.  &X f-^G O£ei "  C^>SOE3#3    ISC

Date and time of wt. (o'/^'8(   O
                                                       (o?4#3-4>
                                                              - 8
                                                               - /
                                                            3. /
                                                              mg "

                                                             . mg*-
 mg •

. mg ••



. mg "

. mg "

. nig ^

. mg-

.mg "



 mg%'

 mg-
     Signature of reviewer
                               C-22

-------
         METHOD 5 TRAIN ANALYTICAL PARTICULATE  DATA
Plant
                     3526-/7
                                               Run  No.
Sample location 	
Relative humidity  5o°/g
Density of acetone  (pa)
                                                      g/ml
Sample
type
Acetone rinse
filter (s)
Sample
identifiable
\i^S
*es
Liquid level at mark
and/or container sealed
ve6
ves
Acetone rinse container no. BK
Acetone rinse volume  (Vaw)
                                       55/5 A
                                                   ml
Acetone blank residue concentration
Wa = Ca Vaw pa =  ( ,o'i  )
Date and time of wt  £>-/*?-8/ P'/S/?--^
Date and time of wt  £
                                     (Ca)   .O I
                                       Gross wt
                                       Gross wt
                                                  	 mg/g
                                                  	 mg -•
                                                  7/076-3 mg
                                                  7lQ~JoO«2<^5/ £6
Date and time of wt  6-/7-g/  tf.'iSa^    Gross  wt
Date and time of wt  £-/? -#/  3'3o f>-^   Gross  wt
                               Average  gross  wt
                                         Tare  wt
             Weight of particulate on filter (s)
         Weight of particulate in acetone rinse
                    Total weight of  particulate __ _
Note: In no case shall a blank residue  greater than (.01 mg/g)  or
.001% of the weight of acetone used  be  subtracted from the sample
weight.
                                                    358-8  mg
                                                    350.^  mg
                                                           mg'
                                                    35S.9  mg
                                                      P-7  mg.
                                                      3-S  mg
                                                      /
-------
         METHOD 5 TRAIN ANALYTICAL  PARTICULATE DATA
Plant  U.5.
                    35^5 -/7
                                               Run No.
Sample location
Relative humidity
Density of acetone
                    (pa)
                                                      g/ml
Sample
type
Acetone rinse
filter(s)
Sample
identifiable
V'   ) (i4-c~7  )
Date and time of wt _£^"/^-(§/  3-'-
Date and time of wt  £>
                                          ,O I
                                                         mg/g
                                                         mg "
                                    >    Gross wt  h5S81-(&  mg "
                               6'OOft/w  Gross wt  £>59gc3.o  mg"
                               Average gross wt  65bBI• 8  mg-'
                                         Tare wt  £5 873.0 mg ""
                     Less acetone  blank wt (Wa) 	3-3- mg ~-
         Weight of particulate  in  acetone rinse 	5-b> mg -
Filter (s) container no. g>X <56 ":oood-t2-&
Date
Date
and time of wt 6"/7"8/ ^•'iSa^ Gross wt
and time of wt £?'/?-£/ S-^o^-n Gross wt
Average gross wt
Tare wt
Weight of particulate on filter (s)
Weight of particulate in acetone rinse
Total weight of particulate
36^-5- mg
36^. 5- mg "'
067' 3- mg
366.3- mg^
3-O mg
£>•&? mg v
8' 6 mg -•
Note: In no case shall a blank  residue greater than (.01 mg/g) or
.001% of the weight of acetone  used  be subtracted from the sample
weight.
Remarks:
     Signature of analyst
     Signature of reviewer
                               C-24

-------
METHOD 5 TRAIN ANALYTICAL PARTICULATE DATA
Plant
          35P-5-/7
                                               Run No.
Sample location 	
Relative humidity
Density of acetone  (pa)
                                            g/ml
Sample
type
Acetone rinse
f ilter (s)
Sample
identifiable
N/e.5
X<^
Liquid level at mark
and/or container sealed
v/^S
y^s
Acetone rinse container no.  S>X /76
Acetone rinse volume  (Vaw)   3-8 Q
                                         ml
Acetone blank residue concentration
Wa = Ca Vaw pa =  ( . O /  ) ( P-S?  )
Date and time of wt  6~/?'8/
Date and time of wt  (o
                                     (Ca)
                                      )  =
                                          . PI
                                               mg/g "
                                               mg  -
                              Gross wt  fo(eC)&Q.(p mg -
                              Gross wt  66£?£ffi.£)  mg "
                      Average gross wt  (?&>0&'8.8 mg -
                                        Tare wt
                     Less acetone blank wt  (Wa)
         Weight of particulate in acetone rinse
Filter (s) container no. £>)(./57 ^QOoZ-iSl ($£>3~(p8) •
                                       Gross wt
                                       Gross wt
                                                  mg-
                                                  mg
                                                  mg
                                                      /.O
Date and time of wt  6'/?-gy  ^
Date and time of wt  ic'll'&i  ^:^Op<-
                               Average  gross  wt
                                         Tare  wt
             Weight  of particulate on filter (s)
         Weight of particulate in acetone  rinse
                     Total weight of  particulate
Note: In no case shall a blank residue  greater than (.01 mg/g)  or
.001% of the weight  of acetone used  be  subtracted from the sample
weight.
Remarks:
                                                  mg -'
                                                  mg *•
                                                  mg •'
                                                  mg *''
     Signature of analyst
     Signature of reviewer
                                              f-
                                              r
                                                A A
                     C-25

-------
                                                         Page  1  of 2
             Analytical  Organic  Particulate Data
Plant
                     35»5-/7
                                              Run No .
Sample location
Relative humidity
Density of acetone  (pa)
                                                        g/ml
Sample
type
Acetone rinse
Impinger rinse
Filter (s)
Sample
identifiable
>/e5
/*<,
y-s
Liquid level at mark
and/or container sealed
y
Date and time of wt. £-/?-?<

Date and time of wt. &~/7'ft
                               */-.'3o
                                         Gross wt.

                                         Gross wt .
                                Average gross wt.

                                          Tare wt.

              Weight of particulate  on  filter (s).

           Weight of particulate  in  acetone rinse.

                      Total weight of particulate.

                               FRONT  HALF SUBTOTAL,




                               C-26
                                                         36g*/-.Q
 mg (s
    /'


 mq>/

 mg^

. mg''




 mg ^'

-------
                                                         Page 2 of 2
BACK HALF ETHER-CHLOROFORM EXTRACTION

Impinger contents and  water wash of
 impingers, connectors,  and back             ,             .
 half of filter holder.   Container nn. BX >Lr I   C SS3O/9-)
Inorganic fraction  container no.

Date and time of wt.  D p^. Gross  wt.     lOOSIk-i   mg-

Average gross  wt.	/gof?^^.^  mg-^

         Tare  wt.	/£o£>&8-fc  mg »-
                              Less water blank wt.

                 Total  weight of inorganic phase

Organic fraction container  no.  p)C /H"~7 ''

Date and time of wt.  fc'ltf'tfl tf'OO ^U-^ Gross wt._

Date and time of wt. (c'cr-v-'ol  K>.OOc*r>-^ Gross wt._

   i.Oi)  C/t> j C >cn   -  l<(
-------
         METHOD 5 TRAIN ANALYTICAL PARTICULATE DATA
Plant
                     35P6-/7
Run No.
Sample location 	
Relative humidity
Density of acetone  (pa)   -7*9 g) =  /-I
Date and time of wt   6"/"?'3/  7-**fSrf~> Gross wt
Date and time of wt   &~rf~8i  «^'/5/?o-. Gross wt
                               Average gross wt
                                        Tare wt
                     Less acetone blank wt  (Wa)
         Weight of particulate in acetone rinse
Filter(s) container no.  £X
                                                         mg/g-
                                                         mg '
                                                        0_ mg-^
                                                        S_ mg "
                                                        3i mg-
                                                       /•/
                                                           mg-
time of wt £-/?-#/ tf.'/S&r* Gross wt
time of wt £j-77-$/ 3-'3o^>7 Gross wt
Average gross wt
Tare wt
Weight of particulate on filter (s)
Weight of particulate in acetone rinse
Total weight of particulate
2>fo2>-5 mg
3fo-5- Q mg
3C?3'(p mg
3^7-5 mg
7-8 mg
£>•
-------
         METHOD  5  TRAIN  ANALYTICAL PARTICULATE DATA
Plant   g.6.  LPf\
                                               Run No.
Sample location 	
Relative humidity
Density of acetone (pa)   • ~)1O Q
                                                      g/ml
Sample
type
Acetone rinse
filter(s)
Sample
identifiable
y£5
V^-5
Liquid level at mark
and/or container sealed
^
y^S
Acetone rinse container no.
Acetone rinse volume  (Vaw)
                              £>X I~7B
                                                   ml-
                                           .01
Acetone blank residue concentration  (Ca)  	
Wa = Ca Vaw pa =  ( -6l  ) (3~o$  ) (-"?
Date and time of wt  (c'l'i-Ql l^^g^   Gross wt
Date and time of wt  (c'tf'&l 
-.   Gross wt
                               Average  gross wt
                                        Tare wt
                     Less acetone  blank wt (Wa)
         Weight of particulate in  acetone rinse
Filter (s) container no.  £X 163 *oooJ/37 (S^ci^)  *
Date and time of wt   &>-/7~8l   ^•'I'Sa^   Gross wt
Date and time of wt
                                                        1
                                                         mg/g -'
                                                         mg ^
                                                           mg *
                                                           mg'
                                                           mg •-'
                                                           mg-
                                                           mg •'
                                                           mg •
                       "/ 7 - 8 1  5-
                                        Gross wt
                                Average gross wt
                                         Tare wt
             Weight of particulate on filter (s)
         V7eight of particulate  in  acetone rinse
                    Total weight of particulate
mgr

mg •'"
mg ^
mg •
mg /
Note: In no case shall a blank  residue greater than (.01 mg/g) or
.001% of the weight of acetone  used  be subtracted from the sample
weight.
Remarks:

Signature of analyst (
Signature of reviewer
^IJLAjA/L Y^"H£-.S
,/6"( -^ v/V,/v A_c7,(

7

i .'
', V
                                C-29

-------
         METHOD 5 TRAIN ANALYTICAL PARTICULATE DATA
Plant  U.S.
                   3SAS-/7
       Run No.
Sample location 	
Relative humidity 	
Density of acetone  (pa)
                                                     g/ml
Sample
type
Acetone rinse
filter(s)
Sample
identifiable
V<0
y^
Liquid level at mark
and/or container sealed
veS
t£S
Acetone rinse container no.
Acetone rinse volume  (Vaw)
                                                  ml
Acetone blank residue concentration  (Ca)   .o (
Wa = Ca Vaw pa =  ( ,bt ) ( ^/'P- ) (.~Me%) =   3-3
Date and time of wt 	<£
Date and time of wt   £
                                       Gross wt
                    	 Gross wt
                               Average gross wt
                                        Tare wt
                     Less acetone blank wt  (Wa)
         Weight of particulate in acetone rinse
Filter (s) container no. g>X
Date and time of wt  6~/7~j
Date and time of wt  6-/7-F
                 mg/g -
                 mg -
                l_ mg-
                (& mg •
                                                      3-3
                                        (6$o
-------
         METHOD 5 TRAIN ANALYTICAL PARTICULATE DATA
Plant
                                               Run No.
Sample location
Relative humidity £0
Density of acetone  (pa)
                                                      g/ml
Sample
type
Acetone rinse
filter(s)
Sample
identifiable
V£!>
ye^
Liquid level at mark
and/or container sealed
yes
y^S
Acetone rinse container no.
Acetone rinse volume  (Vaw)
                             £>X / ?£)   5f> / 8 /}
                                                  ml --
Acetone blank residue concentration  (Ca)
Wa = Ca Vaw pa =  ( . c |  ) (
                                           . Dt
Date and time of wt
Date and time of wt
                                       Gross wt
                 mg/g
                 mg ->
                   mg
                             3
Gross wt  (0~l&o€>-\
                               Average  gross  wt
                                                          mg
                                        Tare wt  67?F^.8  mg
                                                          mg
                                                      /3-3L  mg "
                                                           mg
                                                           mg
                                                   3S4-.4- mg
                     Less acetone blank wt  (Wa)
         Weight of particulate  in acetone rinse
Filter (s) container no.  BX/6/ *QooS&93.(S'5t&(3> V
Date and time of wt  fc-/7-ff/  rf'/Sa^  Gross wt
Date and time of wt  (?~/7-&l Ib'-bOp^  Gross wt
                                Average gross wt
                                        Tare wt
             Weight of particulate on filter(s)
         Weight of particulate  in acetone rinse
                    Total weight of particulate
Note: In no case shall a blank  residue greater than (.01 mg/g)  or
.001% of the weight of acetone  used be subtracted from the sample
weight.
Remarks:
                                                      3-5  mg -
                                                      '3-3-  mg ^
                                                      /6.7  mg ^
     Signature of analyst
     Signature of reviewer
                                 /I
                                 /I
                                 C-31

-------
                                                        Page 1 of 2
             Analytical Organic Particulate Data
Plant
                    35.35- J 7
                                             Run No.
Sample location
Relative humidity
Density of acetone (pa)
                                                       g/ml
Sample
type
Acetone rinse
Impinger rinse
Filter (s)
Sample
identifiable
y^s
y^s
ye$"
Liquid level at
and/or container
mark
sealed
y-S
*eS
y*S
FRONT HALF

Acetone wash of nozzle, probe, cyclone
 (bypass),  flask, front half of filter
 holder.      Container no.   E>X. /^^   C56^f
                                                    f4O
Date and
Date and
(.0/3
Filter (s)
Date and
Date and
time of wt. &'2-3-~i ' &Oa^~^ Gross wt.
' Average gross wt.
Tare wt.
Less acetone blank wt. (Wa )
Weight of particulate in acetone rinse
i container no. BX '3k? C^^-^-f-B^ tt OOO 1^1
time of wt. &~H-$( *f- 3 O /?.•»> Gross wt.
time of wt. fe'll'st ^>3o G'->-* Gross wt .
Average gross wt.
Tare wt.
Weight of particulate on filter (s)
Weiqht of particulate in acetone rinse
Total weight of particulate
FRONT HALF SUBTOTAL
97//7-S ma.
oj5.(e> mq •
3S8'5 mg^
2,53,  ij • o jflq i^
^"•^ mg .'
lc)-.(0 mq.
'^•^ mq^'
If'Cc mq1
                             C-32

-------
                                                          Paqe 2 of 2
BACK HALF  ETHER-CHLOROFORM EXTRACTION

Impinger contents and water wash of
 impingers,  connectors,  and back        ^
 half of filter  holder.   Container no.  P*
Inorganic  fraction container no.  C>X /4-jr
Date and time of wt.  (c^/l-fl   1-QOd^ Gross  wt..

Date and time of wt.  -oOci--*-^ Gross  wt..

                       '-  /•£> '   Average gross  wt..

                                          Tare  wt.
Date and time  of  wt.  fe»'^^-r'  Y-3D/>~^  Gross  wt.     y2>C>a^^  Gross  wt.	

                       •' '  i'*> J  Average  gross  wt.	
                                           Tare  wt.	'VgtQOO-/  mg'

                              Less water blank  wt.	T'5"   mg'

                  Total  weight of inorganic  phase 	_£_£___ mg"

Organic fraction  container no.   SX. l^tf ''c?>^
-------
Plant
         METHOD 5 TRAIN ANALYTICAL  PARTICULATE DATA
                                               Run No.
Sample location 	
Relative humidity
Density of acetone
                    (pa)
                                                      g/ml
Sample
type
Acetone rinse
filter (s)
Sample
identifiable
ves
y«-S
Liquid level at mark
and/or container sealed
V^5
ye<,
Acetone rinse container no.
Acetone rinse volume  (Vaw)
                                                   ml
                                          . O /
Acetone blank residue concentration  (Ca)
Wa = Ca Vaw pa =  ( . e>/   ) ( 3M3- ) (.9<7cg)  =   /.^	 m
Date and time of wt  (c'll'Sl  £• l5f>->~>    Gross wt  656^.*j-
Date and time of wt   fe
                                                         mg/g
                                        Gross wt
                               Average  gross wt
                                         Tare wt
                     Less acetone  blank wt (Wa)
         Weight of particulate in  acetone rinse
Filter(s) container no.  gK /66 ^0^0^303 (5-/7'fi /  3-'l5t>S. I mg '
355. i
365- /
mg-
mg '
35
-------
         METHOD  5 TRAIN ANALYTICAL PARTICULATE DATA
Plant   #.5>.   ) (-~H°£ )  =
Date and time of wt  (p-'tf^Bl 3-- l$p^    Gross wt 6^558.0  mg u"
Date and time of wt  (c'9-2~8i  B-OQg--^.   Gross wt (ctfSSQ-Q  mg "'
                                Average  gross wt . I  mg
container no. ?>X I&? ^c&o^-tfti &i-b&0) ^
time of wt Gy-n-Bl ^//Sa^ Gross wt
time of wt 6-/?-g< 3.'3(9p,->^ Gross wt
Average gross wt
Tare wt
Weight of particulate on filter (s)
VJeight of particulate in acetone rinse
Total weight of particulate
3^ • *f- mg -
bicl-^ mg •
2>b I •& mg ^
7«(tf mg ^
(y . / mg -
/3- 7 mg y
Note: In no case shall a blank  residue greater than (.01 mg/g) or
.001% of the weight of acetone  used  be subtracted from the sample
weight.
Remarks:
     Signature of analyst
     Signature of reviewer
                                 C-35

-------
         METHOD 5 TRAIN ANALYTICAL PARTICULATE  DATA
Plant  U -6.
                      35^5 '/7
Run No.
Sample location 	
Relative humidity
Density of acetone  (pa)
                                                      g/ml
Sample
type
Acetone rinse
filter (s)
Sample
identifiable
X^S
y^s
Liquid level at mark
and/or container sealed
yc-s
y^
Acetone rinse container no.
Acetone rinse volume  (Vaw)
                             307
Acetone blank residue concentration  (Ca)  .O\
Wa = Ca Vaw pa =  ( .C '  ) ( 3o'l  ) (
Date and time of wt 	(c'l1'&(  '2-'-
Date and time of wt  6
                                                         mg/g '•'
                                                         mg ---'
                                        Gross  wt 6?7fe>7/?.4,  mg
                                        Gross  wt £>768°-P  mg
                               Average  gross  wt fo~7d>'7£J'B  mg
                                         Tare  wt (07<0~?2-O  mg

Less acetone blank wt (Wa)
Weight of particulate in acetone rinse
P. 4- mg 3) ^
Date
Date
and time of wt 6 -/?-$/ £)><5~2>Cp^ Gross wt
Average gross wt
Tare wt
Weight of particulate on filter (s)
Weight of particulate in acetone rinse
Total weight of particulate
3 ^ ? - o mg *
3S7- / mg -'
357-O mg -
5S*/--<^- mg"
<2--(e mg s
S'<4- mg y
8,O mg ^
Note: In no case shall a blank  residue  greater than (.01 mg/g) or
.001% of the weight of acetone  used  be  subtracted from the sample
weight.
Remarks:
     Signature of analyst
     Signature of reviewer
                                      ^VL^
                                 C-36

-------
                                                        Page 1 of 2
             Analytical Organic  Particulate Data
Plant
Run No. CDP'I
Sample location
Relative humidity    SO C^
Density of acetone  (pa)
          g/ml
Sample
type
Acetone rinse
Impinger rinse
Filter (s)
Sample
identifiable
^S
y a *\
v e j
Liquid level at mark
and/or container sealed
y^S
V- ^-S
V^,S
FRONT HALF

Acetone wash of nozzle, probe, cyclone
 (bypass), flask, front half of filter
 holder.      Container no.  BX /*fS
                              Tare wt.

   Weight of particulate on filter  (s).

Weight of particulate in acetone rinse.

           Total weight of particulate.

                   FRONT HALF SUBTOTAL.




                       C-37
Date and time of wt. (£>~/7'8'
Date and time of wt . (z <3-2'&l
t.oHonc.w,**,
' T.OO^-^ iross wt. '
g.'iO&^ Gross wt.
Average gross wt.
Tare wt.
Less acetone blank wt. (Wa )
Weight of particulat
Filter (s) container no. J3K /3^
Date and time of wt. <£7~/7~8/
Date and time of wt. G?~/')-£>t

e in acetone rinse
? "00&3-3-5S C.'3o#^>-. Gross wt.
^'SOjo-^ Gross wt.
Average gross wt.
OQ^3-2>.( ma"
/Og^^.4, nqu
IOQ^}.& mg^
I0840Z.S ma-
°^ '^- ma -^
/<^ -1 ma i"
6) ^x
3'SS>.<7 mq"
2,55.^ ma.
355.8 mq^
                                                         55^-.^-
              / • 6
                                                           /
-------
                                                         Paqe 2 of 2
BACK HALF ETHER-CHLOROFORM  EXTRACTION

Impinger contents and water wash  of
 impingers, connectors, and back
 half of filter holder.  Container  nn.
Inorganic fraction container  no.   D^  / 5 / "<

Date and time of wt.  &~l~i-)ft  '•{.Qo^-^   Gross wt..

Date and time of wt.  £ 'P-3>-V /  ?-3o«»v—.  Gross wt._

                    '  _ J - o.£ ,/  Average gross wt..

                                          Tare wt._

                              Less water blank wt..

                 Total  weight of  inorganic phase

Organic fraction container  no.  5X. ip I no£-f\''	^_

Date and time of wt.  £"Vy'O/  ^'.DGc*^   Gross wt.

Date and time of wt.  ^
                                g. 
-------
            APPENDIX D




SAMPLING AND ANALYTICAL PROCEDURES
              D-l

-------
D-2

-------
             DETERMINATION OF PARTICULATE EMISSIONS


     All particulate samples were collected using an EPA Method

5 sampling train, and Method 5 sampling procedures, as described

in the Federal Register,* were utilized in all cases.


SAMPLING APPARATUS

     The Method 5 sampling train used in these tests was assembled

by PEDCo personnel and meets all design specifications estab-

lished by the Federal EPA.  The sampling apparatus consisted of:

     Nozzle - Stainless steel  (316) with sharp, tapered leading
     edge and accurately measured round opening.

     Probe - Borosilicate glass with a heating system capable of
     maintaining a minimum gas temperature of 121°C  (250°F) at
     the exit end during sampling.

     Pitot Tube - Type S pitot tube that met all geometry stan-
     dards was attached to probe to monitor stack gas velocity.

     Temperature Gauge - Iron/constantan type-K thermocouple  (or
     equivalent) attached to the pitot tube in an interference-
     free arrangement with a digital readout to monitor stack
     gas temperature within 2.8°C  (5°F).

     Filter Holder - Pyrex glass with heating system capable of
     maintaining a filter temperature of approximately 121°C
     (250°F).

     Filter - 87 mm (3 in.) diameter, glass fiber filter (Reeve
     Angel 934 AH).

     Draft Gauge - An inclined manometer made by Dwyer with a
     readability of 0.25 mm (0.01 in.) H~0 in the 0-250 mm
     (0-10 in.) range was used.
 40 CFR 60,  Appendix A, Method 5, July 1, 1980.

                              D-3

-------
     Impingers - Four Greenburg-Smith design impingers connected
     in series with glass ball joints.  The first, third, and
     fourth impingers were modified by removing the tip and ex-
     tending the tube to within 1.3 cm  (0.5 in.) of the bottom of
     the flask.

     Metering System - Vacuum gauge, leak-free pump, thermometers
     capable of measuring temperature to within 2.8°C  (5°F),
     calibrated dry gas meter, and related equipment, to main-
     tain an isokinetic sampling rate and to determine sample
     volume.  The dry gas meter is made by Rockwell and the
     fiber vane pump is made by Cast.

     Barometer - Aneroid tube type to measure atmospheric pres-
     sures to 0.3 kPa (+0.1 in. Hg).
SAMPLING PROCEDURE

     After selecting the sampling site and the minimum number of

traverse points, the stack pressure, temperature, moisture con-

tent, and range of velocity head were measured according to

procedures described in the Federal Register.*

     Approximately 200 grams of silica gel were weighed and

placed in a sealed impinger prior to each test.  Glass fiber

filters were desiccated for at least 24 hours and weighed to the

nearest 0.1 mg on an analytical balance.  One hundred ml of

distilled water were placed in each of the first two impingers;

the third impinger was initially empty; and the impinger con-

taining the silica gel was placed next in series.  The train was

set up with the probe as shown in Figures D-l or D-la.  The

sampling train was leak checked at the sampling site prior to

each test run by plugging the inlet to the nozzle and pulling a

50 kPa (15 in. Hg) vacuum, and at the conclusion of the test by

plugging the inlet to the nozzle and pulling a vacuum equal to

the highest vacuum reached during the test run.
*
 40 CFR 60, Appendix A, Methods 1, 2, 3, or 4, July 1, 1980.

                              D-4

-------
                                           THERMOMETER
o
ui
              PROBE

            NOZZLE!
                           "S"  1YPL
                             PITOI
                             TUBE li^


                             MANOMETER
                                                HERMOMETER
            CALIBRATED ORIFICE
THERMOMETERS


  V^  V^       ^CONTROL
               MANOMETER
                                    Figure D-l.  Particulate sample train.

-------
o
i
                                       HEATED  AREA


                              STACK WALL
                        FILTER  HOLDER
                                                           THERMOMETER
               PITOT TUBE
                                                                         ICE WATER BATH


                                                                     100 ml  OF  WATER
     THERMOMETER




ORIFICE
BY-PASS

 VALVE
                                                                                  VACUUM GAUGE
                                                              VACUUM LINE
                                                                 VACUUM PUMP
                                      Figure  D-la.   Particulate sampling train.

-------
     The pitot tube and lines were leak checked at the test site

prior to each test run and at the conclusion of each test run.

The check was made by blowing into the impact opening of the

pitot tube until 7.6 cm (3 in.) or more of water were recorded on

the manometer and then capping the impact opening and holding it

for 15 seconds to assure it was leak free.  The static pressure

side of the pitot tube was leak checked using the same procedure,

except suction was used to obtain the 7.6 cm (3 in.) H~0 manom-

eter reading.  Crushed ice was placed around the impingers to

keep the temperature of the gases leaving the last impinger at

20°C (68°F) or less.

     During sampling, stack gas and sampling train data were

recorded at each sampling point and when significant changes in

stack flow conditions occurred.  Isokinetic sampling rates were

set throughout the sampling period with the aid of a nomograph or

programmable calculator.  All sampling data were recorded on the

Particulate Field Data Sheet.


SAMPLE RECOVERY PROCEDURE

     The sampling train was moved carefully from the test site to

the cleanup area.  The volume of distilled water from the first

three impingers was measured.  Sample fractions were recovered as

follows:

     Container No. 1 - The filter was removed from its holder and
     placed in a petri dish and sealed.

     Container No. 2 - Loose particulate and acetone washings
     from all sample-exposed surfaces prior to the filter were
     placed in a polyethylene jar, sealed, and labeled.  Par-
     ticulate was removed from the probe with the aid of a


                               D-7

-------
     brush and acetone rinsing.   The liquid level was marked
     after the container was sealed.

     Container No.  3 - A minimum of 200 ml of acetone was taken
     for the blank analysis.  The blank was obtained and treated
     in a similar manner as the  acetone washing.

     Contaner No. 4 - After being measured, distilled water in
     the impinger section of the sampling train was placed in a
     polyethylene container.  The impingers and connecting
     glassware were rinsed with  distilled H20 and this rinse was
     added to the container for  shipment to the laboratory.

     Container No.  5 - A minimum of 200 ml of distilled water was
     taken for the blank analysis.  The blank was obtained and
     treated in a similar manner as the water rinse.

     Container No.  6 - An unused glass fiber filter was taken
     for blank analysis.

     The silica gel from the fourth impinger was weighed and

recorded on the Sample Recovery  and Integrity Data Sheet with

other pertinent data.


ANALYTICAL PROCEDURES

     The following procedures were used and follow the methods

described in the Federal Register.*

     Container No.  1 - The filter and any loose particulate
     matter from this sample container were placed into a tared
     glass weighing dish, desiccated for 24 hours to a constant
     weight, and weighed to the  nearest 0.1 mg.

     Container No.  2 - The acetone washings were transferred to a
     tared beaker and evaporated to dryness at ambient tempera-
     ture and pressure, desiccated for 24 hours to a constant
     weight, and weighed to the  nearest 0.1 mg.

     Container No.  3 - The acetone blank was transferred to a
     tared beaker and evaporated to dryness at ambient tempera-
     ture and pressure.  The blank was then desiccated for 24
     hours to a constant weight and weighed to the nearest 0.1
     mg.
 40 CFR 60, Appendix A, July 1, 1980,
                              D-8

-------
     Container No. 4 - The volume of distilled water and water
     rinse was measured and transferred to a separatory funnel.
     The sample was extracted three times with diethyl ether,
     each time draining the water back into the original sample
     container and the ether into a clean, tared beaker.  The
     sample was then extracted three times with chloroform,
     each time draining the chloroform into the beaker with the
     ether.  After the final extraction, the water portion was
     drained into a separate tared beaker, evaporated to dryness
     at 105°C, desiccated, and weighed to a constant weight to
     obtain the condensible inorganic content.  The ether/chloro-
     form portion was evaporated to dryness at ambient tempera-
     ture, desiccated, and weighed to a constant weight to ob-
     tain the condensible organic content.

     Container No. 5 - The distilled water blank was transferred
     to a tared beaker and evaporated to dryness at 105°C.  The
     blank was then desiccated to a constant weight and weighed
     on an analytical balance to the nearest 0.1 mg.

     Container No. 6 - The unused glass fiber filter was treated
     in an identical manner as the filter in Container No. 1.

     The term "constant weight" means a difference of no more

than 0.5 mg or 1 percent of total weight less tare weight, which-

ever is greater between two consecutive readings, with no less

than 6 hours of desiccation between weighings.  All analytical

data are recorded on the Analytical Particulate Data Sheet.

Acetone and water blank data are recorded on respective blank

data sheets.
                               D-9

-------
                 DETERMINATION OF LEAD EMISSIONS


     All particulate samples were collected using an EPA Method

5 sampling train, and Method 5 sampling procedures, as described

in the Federal Register,* were utilized in all cases.


SAMPLING APPARATUS

     The Method 5 sampling train used in these tests was assembled

by PEDCo personnel and meets all design specifications estab-

lished by the Federal EPA.  The sampling apparatus consisted of:

     Nozzle - Stainless steel  (316)  with sharp, tapered leading
     edge and accurately measured round opening.

     Probe - Borosilicate glass with a heating system capable of
     maintaining a minimum gas temperature of 121°C  (250°F) at
     the exit end during sampling.

     Pitot Tube - Type S pitot tube that met all geometry  stan-
     dards was attached to probe to monitor stack gas velocity.

     Temperature Gauge - Iron/constantan type-K thermocouple  (or
     equivalent) attached to the pitot tube in an interference-
     free arrangement with a digital readout to monitor stack
     gas temperature within 2.8°C (5°F).

     Filter Holder - Pyrex glass with heating system capable of
     maintaining a filter temperature of approximately 121°C
      (250°F).

     Filter - 87 mm  (3 in.) diameter, glass fiber filter  (Reeve
     Angel 934 AH).

     Draft Gauge - An inclined manometer made by Dwyer with a
     readability of  0.25 mm  (0.01 in.) H20 in the 0-250 mm
      (0-10 in.) range was used.
 Federal Register, Vol. 45, No.  9, January  14,  1?80
                               D-10

-------
     Impingers - Four Greenburg-Smith design impingers connected
     in series with glass ball joints.  The first, third, and
     fourth impingers were modified by removing the tip and ex-
     tending the tube to within 1.3 cm (0.5 in.) of the bottom of
     the flask.

     Metering System - Vacuum gauge, leak-free pump, thermometers
     capable of measuring temperature to within 2.8°C (5°F),
     calibrated dry gas meter, and related equipment, to main-
     tain an isokinetic sampling rate and to determine sample
     volume.  The dry gas meter is made by Rockwell and the
     fiber vane pump is made by Cast.

     Barometer - Aneroid tube type to measure atmospheric pres-
     sures to 0.3 kPa  (+0.1 in. Hg).
SAMPLING PROCEDURE

     After selecting the sampling site and the minimum number of

traverse points, the stack pressure, temperature, moisture con-

tent, and range of velocity head were measured according to

procedures described in the Federal Register.*

     Approximately 200 grams of silica gel were weighed and

placed in a sealed impinger prior to each test.  Glass fiber

filters were desiccated for at least 24 hours and weighed to the

nearest 0.1 mg on an analytical balance.  One hundred ml of 0.1 N

nitric acid were placed in each of the first two inpingers^

the third impinger was initially empty; and the impinger con-

taining the silica gel was placed next in series.  The train was

set up with the probe as shown in Figures D-2 or D-2a.  The

sampling train was leak checked at the sampling site prior to

each test run by plugging the inlet to the nozzle and pulling a

50 kPa (15 in. Hg) vacuum, and at the conclusion of the test by

plugging the inlet to the nozzle and pulling a vacuum equal to

the highest vacuum reached during the test run.
 40 CFR 60, Appendix A, Methods 1, 2, 3, or 4, July 1, 1980.

                               D-ll

-------
                                        THERMOMETER
o
I
M
ro
               PROBE
             NOZZLEI
                          STACK  WALL
"S" 1YPL
 PITOT
  TUliC
                            MANOMETER
                                                                        HERMOMETER
             CALIBRATEO ORIFICE
               MANOMETER
    THERMOMETERS
      oo
                                   Figure D-2.  Lead sampling train.

-------
o
i
M
OJ
                                         HEATED AREA


                                STACK WALL
                        'FILTER HOLDER
                                                           THERMOMETER
              NOZZLE^
i
^N\1

-v ' 	 	
>
' TUBE s|x
1

PROBE


*M
-------
     The pitot tube and lines were leak checked at the test site

prior to each test run and at the conclusion of each test run.

The check was made by blowing into the impact opening of the

pitot tube until 7.6 cm (3 in.)  or more of water were recorded on

the manometer and then capping the impact opening and holding it

for 15 seconds to assure it was leak free.  The static pressure

side of the pitot tube was leak checked using the same procedure,

except suction was used to obtain the 7.6 cm (3 in.) H^O manom-

eter reading.  Crushed ice was placed around the impingers to

keep the temperature of the gases leaving the last impinger at

20°C (68°F) or less.

     During sampling, stack gas and sampling train data were

recorded at each sampling point and when significant changes  in

stack flow conditions occurred.  Isokinetic sampling rates were

set throughout the sampling period with the aid of a nomograph or

programmable calculator.  All sampling data were recorded on  the

Particulate Field Data Sheet.


SAMPLE RECOVERY PROCEDURE

     The sampling train was moved carefully from the test site to

the cleanup area.  The volume of  solution from  the  first three

three impingers was measured.  Sample fractions were recovered as

follows:

     Container No. 1 - The filter was removed from  its holder and
     placed  in a petri dish and sealed.

     Container No. 2 - Loose particulate  and acetone washings
     from  all sample-exposed surfaces prior to  the  filter were
     placed  in a polyethylene container,  sealed, and labeled.  Par-
     ticulate was removed from the probe  with the aid of a
                                D-14

-------
     brush  and  acetone  rinsing.   The  liquid  level  was  marked
     after  the  container  was  sealed.

     Container  No.  3  -  A  minimum of 200  ml of  acetone  was  taken
     for  the  blank  analysis.   The blank  was  obtained and treated
     in a similar manner  as the  acetone  washing.

     Container No.  4  - 0.1 nitric  acid washings of all sample-
     exposed surfaces prior to the filter were placed  in a
     polyethylene container,  sealed,  and labeled.

     Container No.  5  - Nitric acid in the impinger section of
     the sampling train was placed in a polyethylene container.
     The impingers and connecting glassware were rinsed with 0.1
     N nitric acid and this rinse was added to the container for
     shipment to the  laboratory.

     Container No.  6  - A minimum of 200 ml of 0.1 N nitric acid
     was taken for the blank analysis.  The blank was  obtained
     and treated in a similar manner as the nitric acid rinse.

     Container No.  7  - An unused glass fiber filter was taken
     for blank analysis.

     The silica gel from the fourth impinger was weighed and

recorded on the Sample Recovery and Integrity Data Sheet with

other pertinent data.


ANALYTICAL  PROCEDURES

     The following analytical procedures were used:

     Container No.  1  - The filter and any loose particulate
     matter from this sample container were placed into a tared
     glass  weighing dish, desiccated for 24 hours to a constant
     weight,  and weighed to the nearest 0.1 mg.  Following this
     determination, the filter and loose particulate were cut
     into strips and  placed into a 125 ml Erlenmeyer flask.  The
     petri  dish was rinsed with 10 ml of 50 percent HNC>3 to
     insure quantitative recovery of lead.  This rinse is added
     to the flask for lead extraction and analysis.

     Container No.  2  - The acetone rinsings were transferred to
     a tared beaker and evaporated to dryness to a constant
     weight,  and weighed to the nearest 0.1 mg.  Following this
     the residue was  transferred to the Erlenmeyer flask contain-
     ing the sample from Container No. 1 using 30 ml of 50 per-
     cent HN03.
                              D-15

-------
      Container No.  3 - The contents of this container were
      transferred to a beaker and taken to dryness.   Following
      this the residue was transferred to the Erlenmeyer flask
      containing the samples from Containers Nos.  1  and 2 using
      30 ml of 50 percent HN03.

      Container No.  4 - The acetone blank was transferred to a
      beaker and evaporated to dryness to a constant weight,
      and weighed to the nearest 0.1 mg.  The blank  was then
      extracted for  lead and analyzed along with the samples.

      Container No.  5 - The contents were transferred to a beaker,
      and taken to dryness.  This residue was then transferred
      to the Erlenmeyer flask containing the samples from Con-
      tainers Nos. 1, 2, and 3 using 30 ml of 50 percent HN03.

      Container No.  6 - The 0.1 N HNO3 blank was transferred to
      a beaker and taken to dryness.  The blank was  then ex-
      tracted for lead and analyzed along with the samples.


     The term "constant weight" means a difference of no more

than 0.5 mg or 1 percent of total weight less tare weight, which-

ever is greater between two consecutive readings, with no less

than 6 hours of desiccation between weighings.


 LEAD  EXTRACTION

      The  contents of the  Erlenmeyer flask were  heated  for  30 min-

 utes  with periodic  stirring  at  a  temperature  just less  than  boil-

 ing.   Heating  was continued  for  10  minutes  after adding  10 ml  of

 3 percent ^2°2'  and  for  20 more minutes  after adding  50  ml of  hot

 80°C  (176°F) distilled  H2O.   The  sample  was cooled and  filtered
 through a  membrane filter to  remove  particulate matrix  inter-

 ferences.  The filtrate was diluted  to  volume in a 250 ml  volu-

metric flask.  The acetone,  0.1 N HNOj  and  filter blanks were

 separately extracted  in the  same manner.
                               D-16

-------
LEAD ANALYSIS



     The absorbance of each sample fraction and blanks was deter-



mined in triplicate on a calibrated spectrophotometer.  Appro-



priate dilutions were made to bring all sample Pb concentrations



into the linear range of calibration.  The absorbance of each



sample was corrected for blank results, and one sample from each



test site was checked for matrix interferences by a Method of




Standard Additions.  All analytical data were recorded on the



particulate, lead, and blank analytical data sheets.
                               D-17

-------

-------
            APPENDIX E




CALIBRATION PROCEDURES AND RESULTS
                E-l

-------
E-2

-------
               CALIBRATION PROCEDURES AND RESULTS


     All of the equipment used was calibrated according to the

procedures outlined in Maintenance, Calibration, and Operation

of Isokinetic Source-Sampling Equipment.*


NOZZLE DIAMETER

     The nozzles were calibrated by making 3 separate measure-

ments using different inside diameters and calculating the

average.  If a deviation of more than 0.002 inches was found the

nozzle was either discarded or reamed out and remeasured.  A

micrometer was used for measuring.  ^his calibration data is

shown in Figure E-l.


PITOT TUBE CALIBRATION

     The pitot tubes used in sampling were constructed by PEDCo

Environmental and met all requirements of Method 2, Section 4.1

of the Federal Register.**  All pitot tubes were calibrated

before field use according to the Quality Assurance Handbook for

Air Pollution Measurement Systems*** to determine a baseline

coefficient.  See Figures E-2 and E-2a for alignment requirements

of Method 2, and Figure E-3 for actual inspection and calibration
  *
   Office of Air Programs Publication No. APTD-0576
 **
   40 CFR 60, Appendix A, July 1, 1980.
***
   Quality Assurance Handbook for the Air Pollution Measurement
   Systems, Vol. Ill, August 1977.~~	
                              E-3

-------
                    NOZZLE CALIBRATION
Date
where :
                              Calibrated by
M>. rvTZ-6x£^

Nozzle
identification
number

D-i / in.

D~, in.

D3, in.

AD, in.

avg

     AD =
          nozzle  diameter measured on a different  diameter,  in,
          Tolerance  = measure within 0.001  in.

          maximum difference in any two measurements,  in.
          Tolerance  = 0.004 in.
    avg
        = average  of D, ,  D?, and D...
               Figure E-l.  Nozzle calibration  data.
                           E-4

-------
                    NOZZLE  CALIBRATION
Date
        ' &
Calibrated by
j- t
Nozzle
identification
number
4-/0-Z.
i/-/Z2
D,, in.
£XZ^/

D2/ in.
o.z*ft
azsr
D3, in.
p.vSo

AD, in.
£?^?£?z_
0,00 /
D
avg
o.*S»
o.ZSY
where:




Dl 2 3
 ± , Z , _5 ,




     AD





   D
    avg
          nozzle diameter measured  on  a different diameter, in,

          Tolerance = measure within  0.001 in.


          maximum difference in  any two measurements, in.

          Tolerance = 0.004 in.
        = average of D,, D_, and  D_.
                    Figure E-l (continued)
                        E-5

-------
                    NOZZLE  CALIBRATION
Date
                     Calibrated by
Nozzle
identification
number
t-j — • ) | [_/>
$-))!
1-tn
D,, in.
.155
..3)0

D2, in.
<^3o*

where:

Dl 2  3
 j. / ^ , j ,

      AD
  nozzle diameter measured on  a  different diameter, in,
  Tolerance = measure within 0.001  in.

  maximum difference in any two  measurements,  in.
  Tolerance = 0.004 in.
   D
    avg
= average of D,, Dj, and  D_,
                       Figure  E-l (continued)
                             E-6

-------
                    NOZZLE CALIBRATION
Date
-9-3)
Calibrated by
	 '
Nozzle
identification
number
ji 4rr/-_
*-"
D, , in.
— >; q
.z$r
D2, in.
-, c

D3, in.
-i «^
" — rr^ —
• CJ^s 1
AD, in.
s~\^~>

.00 Z
avg
	
- ">/" "^
' ^^> /
where :
D, _ , = nozzle diameter measured on a different diameter, in.
' ' ' Tolerance = measure within 0.001 in.
AD = maximum difference in any two measurements, in.
    avg
          Tolerance = 0.004 in.
        = average of D,, D2, and D_,
                   Figure E-l (continued)
                           E-7

-------
                     NOZZLE CALIBRATION
Date
                      Calibrated by  , / I
V
Nozzle
identification
number
n~ \ * /• ' f~~ "o / — ~~
1 \ v ' " f c *• — '
/ D /, v - / / 6
D,, in.

D2, in.

D3, in.

AD, in.

D
avg

where:
D, = nozzle diameter measured on a different diameter, in.
' ' ' Tolerance = measure within 0.001 in.
AD = maximum difference in any two measurements, in.
   D
    avg
          Tolerance = 0.004 in.
= average of  D, ,  D_,  and D.,.
                     Figure E-l  (continued)
                              E-8

-------
                    NOZZLE CALIBRATION
Date
                     Calibrated  by
Nozzle
identification
number

Z- /&J^Wv
^ - /.- 'i  ' *- •" f — x.

D^, in.
.*sg
,5/6
£,3/^

D2, in.
.*?7
• 3)5"
0,3/3

D3, in.
,a^
.3/5
*.5o-

AD, in.
.e^s
.*o<
^ / cO o 3

avg
.*r.
. 3V -


where:




Dl 2 3
 j., / , j ,




     AD





   D
    avg
  nozzle diameter measured  on  a  different diameter, in,

  Tolerance = measure within 0.001  in.


  maximum difference in any two  measurements,  in.

  Tolerance = 0.004 in.
= average of D,, D_, and D_.
                      Figure E-l (continued)
                             E-9

-------
                    NOZZLE CALIBRATION
Date
 tin It I
Calibrated by
Nozzle
identification
number
-i-iof
Dlf in.
,;oo
D2, in.
,/??
D3/ in.
,rtf-
AD, in.
rjOO/
D
avg
,'ff
where:
AD =
          nozzle diameter measured on  a  different diameter,  in.
          Tolerance = measure within 0.001  in.

          maximum difference in any two  measurements,  in.
          Tolerance = 0.004 in.
   D
    avg
   = average of D,, D~, and D_.
                      Figure E-l (continued)
                            E-10

-------
                 TRANSVERSE
                 TUBE AXIS
                           \
                                     FACE
                                 ~ OPENING ~
                                1    PLANES

                                 (a)  ENDVIEW
                                    A-SIDE  PLANE
   LONGITUDINAL
    TUBE AXIS 0~
       	k_ ^_
	L
                                                           NOTE:
0.48 cm < Dt  <  0.95  cm
(3/16 in.)      (3/8  in.)
                                                    _

                                                     PB
                             ,1.05  Dt  <  P <  1.50 Dt
                                  PA = PB
       B-SIDE  PLANE

      (b)
                                  A or B
                                   (c)
  Figure  E-2.   Properly  constructed  Type  S  pitot  tube,  shown  in:   (a)  end  view;
  face opening  planes  perpendicular  to  transverse axis;  (b) top  view;  face open-
  ing  planes  parallel  to longitudinal axis;  (c) side  view;  both  legs of  equal
  length  and  centerlines coincident, when viewed  from both  sides.   Baseline
  coefficient values of  0.84  may  be  assigned  to pitot tubes constructed  this  way.
                                      E-ll

-------
           TRANSVERSE
            TUBE AXI
    'al /

    !7
RSE   /^
XILJ/    >f^
                            (a)
LONGITUDINAL
TUBE AXIS
\
B
FLOW
t
                (c!
         Bl
                                         (e)
                                    (f)
                                                           B2  (+  or  -)
                                                           Bl ( +  or  -)
Fiqure E-2a.  Types  of  face-opening misalignment that can result from field
use or improper  construction of Type S pitot tubes.  These will not affect
Cp so long as ai  and &2  <10°»  Bl and B2 <5°» z <0.32 (1/8 in.) and w <0.08
cm (1/32 in.).
                                E-12

-------
                 PITOT TUBE INSPECTION  DATA SHEET
o, c _y. u  °  (must be less than  10°)



o- =  "),£>'  (must be less than  10°)



6. =  ft C>  °  (must be less than  5°)



             (n.ust be Jess than  5°)
            inches
2  = A sin  •>  = «C;*>V?y inches  (must be  less  than 0.125 inches)



v  = A sin  r  =j3^y^  inches  (must be  less  than 0.03125 inches;
P_ = M-JS inches
 B


P  = .37*   inches



Pitot tube  No.   fQ/7



Need calibration  	 yes  \/   no



Inspector^ (L^

       /
Date
               Figure E-3.  Pitot tube inspection data sheet.
                               E-13

-------
                       PITOT TUBE CALIBRATION DATA SHEET
Pi tot tube No.:    c? /"7
Reference pi tot tube No.:
                                Date:
                                           Type:
                                                       Calibrator:  G.  A
                                                                        ™
                                                                 Cp:    O>
Side
A
A
A
B
B
B
APstd
1n. HzO
0.^/1
o.32>
6.23
e.Yt
o
o-~f°
e>. 5t>
*.32
Cp(s)
a
c?.83
0.W
0.13
o.%3
o.fo
e>&
Dev.
b
o.ol
CxoZ_
0<0>
0. 0(
0,02.
O.OI

Cp(A)
0-fZ.
Cp(s)
o, «5?Z
5iv.(A)
c
O'Ot

Cp(B)
0.^2.
Bev.(B)
c
O, Of
|Cp(A)-Cp(B)|
c
O, f>&

8 Cp(s) - (CPstd)(APstd/Aps)1/2
b Deviation = |Cp(s)-Cp(A or B)|
c Must be less than or equal to 0.01.
                               Figure  E-3  (continued)
                                    E-14

-------
6  =
                PITOT  TUBE  INSPECTION DATA SHEET




          °  (must be less  than 10°)


          c  (roust be less  than 10°)
        C' °  (must be  less  than 5°)
             (r.ust be  less  than 5°)
A  = f'p'C*-- inches


z  = A sin i


v  = A sin r


          - inches


           inches


           inches
P  =
 B
                      inches (must be less than 0.125  inches)


                      inches (must be less than 0.03125  inches)
P  = , j'


Pitot tube No.  , O3 9-
Need calibration


Inspector


Date //$*>>!£ /
                        yes
                                  no
                         Figure E-3 (continued)
                                E-15

-------
                       PITOT  TUBE CALIBRATION DATA SHEET

P1 tot tube No.:      OS2      Date:  2-A/8f      Calibrator;^
Reference pitot tube No.:
Type:
Cp:   0.
Side
A
A
A
B
B
B
APstd
1n. H20
*.V?
«>-J3
^ 23
0,1*1
*$3
e>, ^"3
Aps
1n. H20
0 73
e.*T?
t>.?
D'tf
Cp(s)
a
tf».«f/
0.1°
t-~go
*.ei
0.10
0*0
Dev.
b
e»
o.^
Cp(s)
o.v^>
Dev. (A)
c
o. &*3

Cp(B)
C?'3
|Cp(A)-Cp(B)|
c
O.oO

8 Cp(s) = (Cpstd)(APstdMps}1/2
  Deviation « (Cp(s)-Cp(A or  B)|
c Must be less than or equal  to 0.01.
                              Figure  E-3  (continued)
                                     E-16

-------
                 P1TOT TUBE INSPECTION DATA SHEET
a. =  /. O  °  (must  be less than 10°)
°5 c  g).C> p  (must  be less than 10°)
6. =  £ .C>  °  (must  be less than 5°)
 1   "^ -
f  =  3 Q  °  (r.-ust  be less than 5r)
e  =
A  =  . =  JQ~) I  inches (must be less  than  0.125 inches)
w  = A sin f =  . C^c-  inches (must be less  than  0.03125 inches)
PA =  -*•!£*•/  inches
pc =  /^-^^ inches
 B
P  = t"37i  inches
Pitot tube No.
Need calibration  _ yes  y^   no
Inspector
Date
                         Figure E-3 (continued)
                                E-17

-------
                       PITOT TUBE CALIBRATION DATA SHEET
F1tot tube No.:      /7?
Date:
7/g/     Calibrator:
Reference pitot tube No.:
           Type:
                     Cp:
Side
A
A
A
B
B
B
APstd
1n. H20
e,i<\
0.-13
0.?~5
*•<>
0.23
Aps
1n. HgO
0,73
b.*i<(
0-31
&.7O
o.«
o.^
Cp(s)
a
e.&l
o.t(
&f(
6.83
£>.*/
o.?<
Dev.
b
o.oo
O.oO
O.OD
<9.0/
0.0)
o.o\

Cp(A)
o.fl
Cp(s)
o.«*
Dev. (A)
c
d>. OO

Cp(B)
c.-rz
Dev.(B)
c
o, o/
|Cp(A)-Cp(B)|
c
0. 0 /

* Cp(s) = (Cpstd)(APstdMps)1/2
b Deviation * |Cp(s)-Cp(A or B)|
c Must be less than or equal to 0.01.
                              Figure E-3 (continued)
                                    E-18

-------
                 PITOT TUBE INSPECTION DATA  SHEET
a.  =  O. °  °  (must  be less than 10°)



a  =  /. O  °  (must  be less than 10°)
   =  J.D
             (must  be  less than 5°)
B  =
           c  (rr.ast  be less thai, 5°)



>  = f. O  °


e  =  /, c>  °


A  = i.o i6 inches


z  = A  sin \  =  &.


w  = A  sin 6  = i?< o i   /
Inspector  p.  *•



Date  ll((/&l
                        yes
                                  no
                         Figure E-3 (continued)
                               E-19

-------
P1tot tube No.:
PITOT TUBE  CALIBRATION DATA SHEET

         Date:   2//(/8/      Calibrator:  $.
                                                                          , L.
Reference pitot  tube No.:     _4~o 2.
                   Type:
3 Cp(s) • (Cpstd)UPstd/Aps)1/2
b Deviation =  |Cp(s)-Cp(A or B)|
c Must be less  than or equal to 0.01.
                            Figure E-3  (continued)
                                                               Cp:   O.
Side
A
A
A
B
B
B
APstd
in. H20
e.z'D
0.37-
^-23
C.&
0
ApS
in. H20
0.-7V
DM7
O. ?«/
c*^
0&
£>.f\
6.JZ-
P>
-------
data of the pitot tubes used during the test program.  Figure



E-4 presents the actual calibration data for each particulate.







DRY GAS METER AND ORIFICE METER




     Figure E-4 was the set-up used for the initial and post-test



calibration.  A wet test meter with a 2-cubic-feet-per-minute



capacity and +1 percent accuracy was used.  The pump was run  for



approximately 15 minutes at an orifice manometer setting of 0.5



inch of water to heat up the pump and wet the interior surface of



the wet test meter.  The information on Figure E-5  (example



calculation sheet) was gathered for the initial calibration and



then, the ratio of accuracy of the wet test meter to the dry  test



meter, and the AH@ were calculated.






POST TEST METER CALIBRATION CHECK



     A post test meter calibration check was made on the meter



box used during the test to check its accuracy against its last



calibration check.  This post test calibration must be within 4^5



percent of the initial calibration.  The initial calibration  was



performed as described in APTD-0576.  The post test calibration



was performed using the same method as the initial calibration.



Three calibration runs were made using the average orifice



setting obtained during each test run and with the vacuum set at



the average value obtained during each test run.  After running



the post test calibration check all three runs were within the +_5



percent range allowed by the Federal Register.*
 *40 CFR 60, Appendix A, July 1, 1980.
                               E-21

-------
            o
                                     /GLASS TUBE
                                    '  THERMOMETER
                         UMBILICAL
METER BOX v^^

                                  PRESSURE
                                  CONTROL
                                  VALVE
                                                              U -  TUBE
                                                             MANOMETER
                                                WET TEST METER
                  Figure E-4.   Calibration setup.
DATE
                                       KETEK BOX HO.
MROHTTRIC
                          in. Kg.
                                       DRY CAS UTTER MO.
Orifice
*anoi»eter
Betting
4H
in. HjO
0. i
i. o
1.5
2.0
3.0
4. 0
Cat volume
wet ten
neter
V ,
w
"3
5
5
10
10
10
10
Gas volume
dry q»6
»eter
V
"3












Wet tot Dry q«> neter
•eter
«W
•F












Inl«t
*«'
•r












outlet
w
•F












Xvrrage
'd'
•r






Tune
6,
• in






1
T






6H?






                                                             Average.

AH

0. S
1.0
l.S
2.0
3.0
4.0

6H
m

0.0366
0. 0137
0.110
0.141
0.221
0.294
t
Vw PK «td « 400)
Va (pb * nri' (tw * 4io>






AH?
0.0317 6H [" ltw* "0) O2
Pfc (ta » 460) [ V^






    V • lUtio ef »ccur«cy of wet t»»t iftetcr  to dry t»»t Mtcr.  Toltrance • + 0.01
  AHf • Orifice of prenure differentiel that give* 0.7S cfm of air at 70*F ant) 2$.92  inch** of
       •ercury, in Hj).   Tolerance • *0.1S.


                Figure E-5.   Calibration  data sheet.


                                  E-22

-------
     The initial and post test meter box calibration data are
presented in Figure E-6.  An on-site field audit was performed
on every metering system before and after the test series.

THERMOCOUPLE
     Thermocouples were calibrated by comparison against an ASTM-
2F thermometer at approximately 32°F, ambient temperature,  100°F,
and 500°F.  The thermocouples read within 1.5 percent of the
reference thermometer throughout the entire range when expressed
in degrees Rankine.  If the thermocouple did not read within 1.5
percent, a correction formula based on a least squares analysis
of the data was utilized.  The correction formula corrected the
data to within 1.5 percent.   The thermocouple was checked at
ambient temperature at the test site to verify the calibration.
Calibration data is presented in Figure E-7.

DIGITAL INDICATOR FOR THERMOCOUPLE READOUT
     A digital indicator was calibrated by feeding a series of
millivolt signals to the input, and comparing the indicator
reading with the reading the signal should have generated.   Error
did not exceed 0.5 percent when the temperatures were expressed
in degrees Rankine.  Calibration data are shown in Figure
E-8.

DRY GAS THERMOMETERS
     The dry gas thermometers were calibrated by comparison
against an ASTM-2F thermometer at approximately 32°F, at ambient
temperature, and at approximately 110°F.  The thermometer agreed
                               E-23

-------
                        MY 6AS METER AND ORIFICE CALIBRATION DATA SHEET
          LEAK CHECK:

          POSITIVE*:
NEGATIVE**:   vacuum used

DATE  ^5~7>.
                                              /7J leakage rate_
                                               METER BOX NO.
          BAROMETRIC PRESSURE, Pfc • .**? *°  In. Hg.   CALIBRATOR,

          VACUUM USED DURING CALIBRATION	  ''I " ^
    trtfict
   MMMler
    •tting
     AN
       to velum*
        «*ttnt
         •eter
                        •Wttr
                         V
                                         Wtitin
Mtttr
 V
           Dry l« mttcr
    Inlet
    V
Outlet
 V
Average
Time
 e,

•in.
    IS
                                                             Gl
    1.0
                                                            AY
    1.6
         10
                                     - /C-C?
                                                          •72
                                                                   7?
    2.0
         10
                                f y/ .
                                                          7S
                                                                    7?
    1.0
         10
                                                                    77
    4.0
         10
                                                                    ?*/
                                                                        **
                                                                                Avenge
AH
13.8
                                    ffc (t, * 480)
                                     AN
                                                                               AN§>
       M3I7 AN      T

       \  (t, + 480)  L
                                                                      * 480)  6 '
   i-5
  0,0368
                                            3 5.
                                                           •"'    . *".--*    *"NJ
                                                         ^^ *^ £. pt ^_^_^*7r -^jr >*-
                                                                                          j 2 .
                                                                                           J
                                                                                           •J'
   IJ
  1.0737
                    1L
                                                                                  -.
-------
               Odte
               Barometric  pressure, P.
               Meter  Box No.
Plant


P/N
                                                                                                      fr^L  /•/<
               Dry Gas Meter No.
                                           _  7
Project Manager  /7/&^A  //% /^
                          _         x

Pretest Y  	/, ^<3.g	
Test
No.
,
2
j
Or i ( ice
manometer
sett ing,
AH,'
in h.O
s ^
if-
y.r
Gas volume
wet test
meter
ft3
10
10
Kf
Gas volunie
dry gas
meter
V
ft3
18-7. ?£3
2*"
7/.^
~?3 - 5"
Tf.-T"
77 £-
7^ y
Or
Inlet
ld,-
°F
t"~
^Z
5s
9/
y tjas mei
Outlet
ldo'
°F
7
Yi
^
^
l-°
,0^
Yi
Vw Pb (td * 460)
vd(pb * flH \(tw » 460]
, >
ff/2.cx»")^2t. vs ^ (s'y?-t>~)
(d.( -?oYz<7. 7^7^ C S3 2 5"
Post-test y - f,ocj^~
w
 I
NJ
U1
* If  UMrt U Ml; OM iMrmUr Ofl IM *'1 9«t avKr r«er4 IM  IMfwrtlurt under t^


•Mr*.
                                                   )
   I  • wi >O!H«* t4tttn| |krou«n IM •«! t«H Ml«r, ft  .


   »  • U   I        in   hr         dr  l«\t Mitr  f|j

   IB • l«Hwr«tur. of IM 9*1  in IM •*! tftl Mtcr. *f

  t^  • IwcMratur* of IM 1*1*1 ut of IM dry ttvl MUr. 'f
   *l
  I  • It^wrttur* »f Ik* Bull*! •*» of IM dry tell Mltr. 'f
   •
   I  • A«cr*«* lt<^*r«iurt of  IM «•> in IM drr (tvt aiitr, oCKinta by th* <>tr<9< of t   
-------
                        DRY &AS METER AMD ORIFICE CALIBRATION DATA SHEET
          LEAK CHECK:

          POSITIVE*:
NEGATIVE":   wicuutn used    2.7.

DATE   6/2/&I
                                                <*
                                       leakage r«te_£_££^a__cfm«»»
                                               METER BOX NO.
IAROMETR1C  PRESSURE, P
          VACUUM USED DURING CALIBRATION
                                        •//  In. Hg.   CALIBRATOR /?,

    •Hficf
   •inoiMltf
    VTtini
     AH
    h.H20
       6u ralwmt
        •Mttni
         •tier
                        •Wter
                         V
                                         wfl tCTt
                     Mittr
                      V
                                Dry |tt mtttr
Inlrt
V
                                                           So*
Avtragt
Tmw
 e,

•in.
    15
i
                                                                    -7-Z-
                                   Pr.
                                                   7?
                                                               7/7^
    1.0
                                      >  600
                                                    7v.
    1.6
          10
                                                             ere
                                                                  71-0
    2.0
          10
                                     ,  8
                                                                $2.0
                                                                                  /.cv~7
    LO
          10
                                       ooe?
                                                                   77
    4.0
         10
                                                    ?y *
                                    . Z/ 0
                                                                   76
                                                                                Avwtgt
   AH
AH
11.6
                                            4<0)
                                     AH
                                                                               AHt
                                                   M3.7AH
   1.5
  •.0368
                      (JTooo)
                           .  VX  )
                                                              i y/
                                                                            ( ^c..o'  >   J
   IX
  10737
                      (.T. c/o i )  ( ^ Jr.
                                                    . e>3.7)
                                                                d   L(T;if!-^0
   u
  1.110
                      (/o. oco )
                                 ) (5:35.6 )
                                                                           . o
                                                                            JVt.' ) (tf en\  "ji
   2.0
  1.147
                                                            ( 0,
                                                                         . o
                      (9.
                                                                     }    L   (
                                                                                          /c.
            1221
                                       .)   r (3JVQ } (/g>. 7t'3)   I
                                                ( ^ 5, V/ ) _LfVV. Z5l   L   (  /O  c>Jt>  \   J
   4J
  UM
                          ooo )  (j£ y,   )  (5V5O:T)
                                                  (<•?.
                                                        ) (  *To   )    r (^?y.o) (y. yy^-l_
  > • lUtle of accuracy of wet test wter to dry test «eter.
     Tolercnce • » O.OZr
AH» • Orifice of pressure differential  that gives 0.7S cfn of air at 70*F and
     29.92 Inches of Mercury, In. H.O.
     Tolerance • 0.1S.           '

   At least five Inches water pressure.
   MUhln three Inches Mercury of absolute vacuum.
*** Not to ticeed 0.005 cf».
                                            Figure E-6 (continued)
                                                     E-26

-------
            Date
            Barometric pressure,  P   =   ,2%
            Meter Box  No.
            Dry  Gas Meter  No.
.."HQ
Plant
P/N      3S-J1T- /?
Project Manager
Pretest Y     /,
                                                                          „' A    /V4. /^
                                                                                  <      .  -
Test
No.
/
2
3
On f tee
manometer
setting,
AH,'
in HO
6'.- S
^- S
&8
Gas volume
wet test
meter
V
ft3
3.0
•K>
10
10
Gas volume
dry gas
meter
V
ft3
\5T67. £0'
J3-t. TV/
,<^7 ///
.fj;? 3 £5~~
r37.3£z~
tf?,?^0
Temperature
Wet test
Meter
w"
°F
•?y.o
7Y.o
_Z^^>
7/^
-?Y,o
~7
£0
£^
Yi
t,oe~7
I.oi3
\.°ii
Yi
Vw Pb (td * 460)
M'" + m)N * 46°)
/^C oooX^^jV^/fe) ^>-3 /, ^
^^, ooo^ttt. yy X ^^^ T^-
(Jj.ct2i)(-Zti. ?y^ )L->'-- --
^- otx>) 62 s <^-/) ^ r^r. -^
KoluM pttting Ikroufh (M Ml Kvl Mtcr. fl .
              «, • fat •olux pitting Inrouffi (M dry (ttl acKr, fc .
              I  • tMp*r«lur« of  In* 9*1  in In* Ml led orttr. *f
             t   * tcr«9« te*p*r«turt •(  ID* 9*> IK the dry itil •*(tr.  obuincd by  the «»cr«9t of t^  tr«9e r«tio of «ccur«cy of -rl test ncler  to dry ten veter for   t«vt
                      Figure  E-6   (continued)

-------
                       DRY 6AS METER AND ORIFICE CALIBRATION DATA SHEET
         LEAK CHECK:

         POSITIVE':
NEGATIVE":  v«cyum used X*Z t> " n*    leakage
DATE   ff/V?y fc'-'7                   METER BOX NO.	
                         l/^Jn-  Hg.   CALIBRATOR  ^
                                ~u"  //:
                                                                     cfm*
         IAROMETRIC PRESSURE.  P
         VACUUM USED DURING CALIBRATION

    •rtfic*
      •mtnt
       •Mtci
       V_-
                                                   Mtttt
                                                    V
                                                    •
                                                     Pry m intler
                                                        Orttt
                                                        '-c
                                                                          °F
TMW
 e,
•in.
    i.s
                               161-300
                                                  7?  •/
                                                7?
                                                              7<^.^
                                                                                   /.y/
                                 e
                                 8 5~> 76$
                                                                                         y
    1.S
         10
                                  7.
                                                 r
                                                                     /J^
    10
         10
                                                     '/
                             3 o f.
                                                       77
                                                                If
            /.6T3
    10
         10
                                to. o dc-
                                                                 7?
                                                                                   i^y
    4.C
         10
   AH
AH
116
                                          4801
                                    AH
                           WITT'
                                                                           AHC
                                                 M3.7AH
   1.5
  U368
                       -c, o )
           &I737
                                                       Ci*
                                                       ^2--J
                                                       377 fJL
                                                                                      533333
   IJ
  Hit
                                . 75-o">
                                     v")
                                                c3»7K/.3-^
                                                                                   / 3 V2??333 )
                                                                                       0
                                                                                       -r
   u
                                                           oi
                                                                                             /- 7)
   u
  •J21
                                             cj
                                                              c 3 .
                                -V 3
                                  3 H")
  Y • Ratio of accuracy of »et test Mter to dr/ test aeter.
    Tolerance • » 0.02>
AH* • Orifice of pressure differential that gives 0.7S cfm of air at ?0*F and
    29.92 inches of aercur/. In. H.O.
    Tolerance • 0.1S.           *
  •
   At least five Inches water pressure.
   Mlthln tnre* Inchei atrxurjr of tbtolutc »acui»
   •ot U uct«d 0.005 cf»
                                         Figure  E-6 (continued)

                                                  E-28

-------
           Date
           Barometric pressure, P.  =  J^7, fl	"Hg
                                                                                                Plant

                                                                                                P/N
           Meter  Box No.
           Dry Gas  Meter No.
Project Manager

Pretest Y     &.
                                                                                                                          , /   //,, //.7^
Test
No.
f
2.
3
On f ice
manometer
setting,
AH;
in h 0
L.o
l
/ & / 2~ 7?$^
'0 f -2. 7-^~
^t/.^7f
Temperature
Wet test
Meter
w'
°F
73, -2.
?3,-2L
72^1
7 /"
r -?z 2.
Dry gas meter
Inlet
°F
go
€f
g<£
^ -
&B
Outlet
°F
7Y
7^
~7S^~
76
7t
~78
Average0
V
°F
7^. ^
$0.2^
ez.*
Time
0, min.
/.«
6Yz'i.*r«lur* under ttf

•ft*r*:
                                                   .1
                                                                                                                                    Calibrated by     LD
              •  • Ut >oluM p«ttint
                                                      m*lir ,  ft
                                                                                                                                                           Signature
             Vtf • Ul >oluM p«t>IH9  through in* dry 1(11 acttr.  ft
             lv • lMp*r«lur< of lh>  f«s in In* ««t 1*11 mtltr .  *f .
             I.  • l«a|Mr<(ur* of tnt  ml*l gti of tn* tr, t*it Ml«r. •(
             *l
             ltf  • 1*ap*rilur* of Int  Outlet ««i of trie dr/ tctt  wttr. *F.

             t  • A«tr<9* tcapcrtlur* of In* 9 of •*! tctt  nwtrr to dry  ten
                  tolerance • freletl I »O.OS t.

             't • >«roa*trK p/ >r*rttl «< M«d «xrl»t
                  10 k* tta MllMi •«•• •»•* *»r
                                                                            Figure  E-6  (continued)
                                              tt« Itll v«rl»>

-------
                         DRY GAS METER AND ORIFICE  CALIBRATION DATA SHEET
          LEAK CHECK:

          POSITIVE*:
          NEGATIVE**:  v«cuum used    £ 7 sT  /•(<.  leakage rate  g>-ofc2. cfm***

          DATE   *J/*'//8/                   METER BOX NO.
          BAROMETRIC PRESSURE, Pfc -^ ft Ay\n.  Hg.    CALIBRATOR   /?,

          VACUUM USED DURING CALIBRATION          T-Y/  "He.
   Orifice
   •ttini
    AH
   ta.H20
      6« volume
      wvtttst
       •wttr
                         try get
                              r
                           V
Wttttit
 Meter
  V
  °
Dry eet meler
                                                                Inlet    Outlet   Avenge
                     Time
                       e,

                      •in.
    IS
                                    O//..TWO
    1.8
                                                                       So
                                                                                                         1.77
    t.5
        10
                                                                       eo
                                                                       <§•(/
    2.0
        10
                                                                                            . to
    j.0
        10
                                  0<{R, 2.00
                                                                                Zu.t
    4J
        10
                                                      7V, -
                                                                                     Avenge
  AH
AH
116
                                  Vw % 
                                                    U3I7AH
  i-6
1.0368
                                                                 ?.
                                                                   Si
  U
0.0737
                                                                                  L
                                                                                    ooo")
                                                                                               ^T
 T * Ratio of accuracy of net test meter to dry test meter.
    Tolerance • * 0.02y
HB « Orifice of pressure differential that gives 0.75 cfm of air at 70*F and
    29.92 Inches of mercury. In. H.O.
    Tolerance • 0.15.

   At least five Inches water pressure.
*•
   Within three Inches mercury of absolute vacuum.
** Not to exceed 0.005 cfm.

                                              Figure  E-6 (continued)

                                                     E-30

-------
            Date
Barometric pressure. P.

Meter Box No.
                                    */.
Dry  Gas Meter  No.
                                        .AS/A
                                                         "Hg
                                                                                               Plant
Project Manager

Pretest Y
Test
No.
/
-2
J
On f tct
manometer
setting,
AM.'
in h.,0
^/
X/ '
yy
Gas volume
wet test
meter
V
ft3
10
10
10
Gas volume
dry gas
meter
V
ft3
£5-3 3UO
£fc>". <9 /of"
££'^ o /-r"
g-/^..-76> 1
&?2.. 7£/
&e-2- 5^f
Temperature
Wei test
Meter
w'
°F
7^5-
•73^
??.*-
?3,
/o.O
fo.0
Yi
,o'tf
/.oV/
/. ^^ ^~
y<
vw Pb (td * 460)
V./P. + AH \ft + 460\
dVb TTeK- ^
<: /-o. 001)^29. ^x) Cgyj. 7 f
(t. 7/3^d2(i. 7 IIM try 441 wl*r r«orfl (M
              I  • Ui •ttli^H ^• (M Ml Icil •»t»r. "F

             l   • liap*r«lurt «f  tkt mlcl V«t ol IM «ry uu «itr.  '(
                                                                                                                                    Calibrated  by
                                                                                                                                                           Signature
             I   • ti
                       r«tHr( •'  IM •utlcl »

                                 lyft Of IM
                                  •' IM dry ictl •(ttr. *f .

                                 » I* IM 
-------
               THERMOCOUPLE  CALIBRATION DATA SHLLT
Date:
Ambient tempers cure:   75    "r   Bui or..<_• trie pressure:  ^.

Calibrator:  3. A^-oJ^-v      Reference:     A

Reference
point
Nc.
/
.-9

J
V


Source, *
(specify)
z
(
Reference
thermometer
temperature ,
op* * *
75-
3-7
~> '
? l/b
3
L IK
Thcrmocoupl e

temperature ,
Op
7 . '? 7
o ~'~>
Critical test points are  32°,  100°,  and 500°.

   *Source:  1) Ice bath
             2) Ambient
             3) Furnace

  **Percent difference
      Reference_temp.  °F  -  thermocouple temp. °F  , ,nnr
             (Reference temp.  °F + 460°F)         *

        Each percent difference must be less than or equal  to  1.5"

 ***Reference thermometer must be ASTM.

****Correction factor must  be  determined if any percent difference
    is >1.5%.
             Figure E-7.  Thermocouple calibration data sheet.
                               E-32

-------
Date:
               THLRMOCOUrLL CALIBRATION  DATA  SHLLT
Thermocouple No.:
Ambient ter
Calibrator

Reference
point
No.
/
n
3
y
Correction
n-.'era ture :
: B. k,,^\r

Source, *
(specify)
i
<
/
•7
2
3
factor****:
/V" °F Barom
^c. Refer en
J
Rvi erence
thermometer
temperature ,
op***
7^
37
>«• -^
YW J
Slo^c: (. v(^
- O. 2C
- 0 Jj"
? 3y
-7, o<-
Reference
point
No .
/
2
.-?
V
Reference
thermometer
temperature ,
Op
7j"
J7
^/^
yv
Corrected
thermocouple
temperature,
Op
7V
jy
/ 2. 1
VI 7
Difference ,
\**
c. /S
c.^t1
- o. 'a' /
o . i ^
Critical test points are 32°, 100°, and  500°.

   *Source:  1)  Ice bath
             2)  Ambient
             3)  Furnace

  **Percent difference
      Reference temp. °F - thermocouple  temp.  °F    ,
             (Reference temp. °F + 460°F)         x

        Each percent difference must be  less  than or  equal  to 1.5r.

 ***Reference thermometer must be ASTM.

****Correction factor must be determined if any percent  difference
    is >1.5%.
                        Fiqure E-7 (continued)
                                E-33

-------
               THERMOCOUPLE CALIBRATION  DATA SHLLT
Date:
Ambient temperature:

Calibrator:  /?
                              Thermocouple  No.:	\2. i

                             5F  Barometric  pressure:  J?9-S***  " li<

                              Reference :A 5 r/*> - j? /^
Reference
point
No .
/
2
1
V
Source, *
(specify)
*
/
.?
3
Reference
therraometer
temperature ,
op* * *
1^
77
//6
1.5%.
                         Figure E-7 (continued)
                               E-34

-------
               THERMOCOnrLL  CALIBRATION DATA SHLLT
Date:
Ambient temperature :

Calibrator :  (]  ^re^
Thermocouple No.:

  Barometric pressure:  J?9. S°  "  ii'j

Reference:    /
Reference
point
No.
/
2
3
V
Source, *
(specify)
-7
/
3
3
Reference
thermometer
temperature ,
op* * *
71
3^
137
(/£.(.
f ' 1
	 1
Thermocouple
temperature ,
Op
?y
3i
&j
w>±
Difference ,
o 37
" o. 2°
c-, t 7
'} , Vt
Correction factor****:   Slope :   /. ^
            Intercept:  -£". s"

Reference
point
No .
1
2
3
1

Reference
thermometer
temperature ,
7t
?r
117
w

Corrected
thermocouple
temperature ,
Op
7f
3^
I-/0
L_ tf*

Di f f erence ,
5 * *
o.'l'
0-20
-o.sv
C.fO
Critical test points are  32°,  100°,  and  500°.

   *Source:  1) Ice bath
             2) Ambient
             3) Furnace

  **Percent difference
      Reference temp. °F  - thermocouple  temp.  °F
             (Reference temp.  °F +  460°F)         x

        Each percent difference must be  less  than or equal to 1.5rr,

 ***Reference thermometer must be ASTM.

****Correction factor must be determined if any percent difference
    is >1.5%.

                       Figure E-7  (continued)
                             E-35

-------
               THERMOCOUPLE CALIBRATION  DATA  SHLLT
Date:
              I»
Ambient temperature:

Calibrator : £?.
           _P.
                              Thermocouple No.:

                            CI  Barometric pressure :_2^L

                              Reference:

Reference
point
No.
1
2.
7
y
• Reference

Sourer , *
(specify)
2
(
thermometer
temperature ,
op***
73^3
35" 6^
3 7?AO
_? <^cj
- o. if
V/.T
Correction farter****:  Slope: /. /';
                                           Intercept:

Reference
point
Nc.
/
2
3
y
Reference
thermometer
temperature ,
°F
7>7
Corrected
thermocouple
temperature ,
Op


Difference ,
$ **
72 o GO
J^ JT o.^o
Cj /
/ *""/
•^y
/oC> • - C.7Z.
J9J
o./Z,
Critical test points are 32C, 100°, and  50DC.

   *Source:  1) Ice bath
             2) Ambient
             3) Furnace
  **Percent difference
      Reference temp. °F - thermocouple  temp.  °F
             (Reference temp.  °F +  460°F)
                                                  x  100f.

        Each percent difference must be less  than or  equal to 1.5C.

 ***Reference thermometer must be ASTM.

****Correction factor must be determined  if any  percent  difference
    is >1.5%.


                       Figure E-7 (continued)
                             E-36

-------
                       THERMOCOUPLE DIGITAL INDICATOR
                          CALIBRATION DATA SHEET
Date   5V j>&
Indicator No.
                                                   Operator 0. .
Test Point
No.
0
1
2
3
4
Millivolt
signal*
**




Equivalent
temperature,
op*
7/
32.O
158.7
5-38. O
II 86, 6
Digital indicator
temperature reading,
°F
^f
3Z
?o&
*37
1/38
Difference,
%
V. oO
&.0&
0-20
O-lO
£>. 07
Percent difference must be less than or equal  to 0.5%.

Percent difference:

  (Equivalent temperature CR- Digital indicator temperature reading °R)(100%)
                              (Equivalent temperature °R)
Where °R = °F + 460°F
 *See thermocouple digital indicator calibration verification device calibra-
  tion for these values.

**This point is ambient temperature.  The device is off and therefore is
  supplying no signal other than ambient temperature.
             Figure E-8.   Digital  readout calibration data sheet.
                                    E-37

-------
                       THERMOCOUPLE  DIGITAL  INDICATOR
                          CALIBRATION DATA SHEET
Date
Indicator No.
Operator
Test Point
No.
0
1
2
3
4
Millivolt
signal*
**




Equivalent
temperature,
op*
•77. c>
32.0
/?5.7
S3&. &
1/86. 6
Digital indicator
temperature reading,
°F
7/
JZ
2 .I1
0* c>O
£>. -2.0
0-3.0
0.17
Percent difference must be less than or equal  to 0.5%.

Percent difference:

  (Equivalent temperature °R- Digital  indicator temperature reading °R)(100%)
                              (Equivalent temperature °R)
Where °R = °F + 460°F
 *See thennocouple digital indicator calibration verification device calibra-
  tion for these values.

**This point is ambient temperature.  The device is off and therefore is
  supplying no signal  other than ambient temperature.
                           Figure E-8 (continued)
                                   E-38

-------
                       THERMOCOUPLE DIGITAL INDICATOR
                          CALIBRATION DATA SHEET
Date   8/C/Bf	 Indicator No.   2 £2-       Operator & A -^± ^ ~»
Test Point
No.
0
1
2
3
4
Millivolt
signal*
**




Equivalent
temperature,
op*
-?y
32.0
t-20
C.33"
p- /o
£). O^~
Percent difference must be less than or equal  to 0.5%.

Percent difference:

  (Equivalent temperature °R- Digital  indicator temperature  reading  CR)(100/Q
                              (Equivalent temperature   R)
Where °R = °F + 460°F
 *See thermocouple digital  indicator calibration verification  device calibra-
  tion for these values.

**This point is ambient temperature.   The device is  off and  therefore is
  supplying no signal  other than ambient temperature.


                             Figure E-8  (continued)
                                     E-39

-------
                      THERMOCOUPLE DIGITAL INDICATOR
                          CALIBRATION DATA SHEET
Date
Indicator No.
Operator /?.
Lg*£a^
Test Point
No.
0
1
2
3
4
Millivolt
signal*
**




Equivalent
temperature,
op*
-?y
32. 0
rtS.7
s?&-c>
/&£.&
Digital indicator
temperature reading,
°F
-7V
33
Jo/ .
537
It&t,
Difference,
%
O, OD
G.ZO
0.-3JT
o~ io
D, o^
Percent difference must  be  less than or equal to 0.5%.
Percent difference:
  (Equivalent temperature  °R- Digital indicator temperature reading °R)(100°Q
                              (Equivalent temperature °R)
Where °R = °F + 460°F
 *See thermocouple digital  indicator calibration verification device calibra-
  tion for these values.
**This point is ambient temperature.  The device is off and therefore is
  supplying no signal  other than ambient temperature.
                            Figure E-8 (continued)
                                    E-40

-------
               THERMOCOUPLE DIGITAL INDICATOR
               CALIBRATION VERIFICATION DEVICE
                    CALIBRATION DATA SHEET
DEVICE NUMBER
DATE
                    CALIBRATOR £
TEST POINT


    1

    2

    3

    4
MILLIVOLT
                    EQUIVALENT
                 TEMPERATURE °F
                        Figure E-8 (continued)
                                 E-41

-------
within 5°F of the reference thermometer.  The thermometers were



checked prior to each test series at ambient temperature to



verify calibration.  Calibration data are included in Figure



E-9.






TRIP BALANCE



     The trip balance was calibrated by comparison with a Class-S



standard weight and agreed within 0.5 g.  Calibration data are



shown in Figure E-10.






BAROMETER



     The field barometer was calibrated to within 0.1 in. Hg of



an NBS-traceable mercury-in-glass barometer before each test



series.  The field barometer was checked against the mercury-in-



glass barometer after each test series to determine if it read



within 0.2 in. Hg.  If it did not read within 0.2 in. Hg, a



correction factor was determined for the last test series.



Calibration data are included in Figure E-ll.
                               E-42

-------
            DRY GAS THERMOMETER  CALIBRATION DATA  SHEET
                                Thermometer No. :  F&-2,
Date:	/•>//'<. .
             I    j-

Ambient temperature:    x7/^— °F   Barometric pressure: jg S.J? ^  " 11'
Calibrator: /?.
                                Reference:

Reference
point
No .
1
2
3


Source , *
2
1
3
i i
Reference \ Thermometer
thermometer
temperature ,
op* * *
?2.°
22.7
_ /23U

temperature, Difference,
op * *
7/ i.&
23 ^-3
>JL* 3 L
           Figure E-9.  Dry gas thermometer calibration  data sheet.
  *Source:   1)  Ice bath
             2)  Ambient
             3)  Furnace set at approximately 110°F

 **Difference must be less than or  equal to j^5°F.

***Reference thermometer must be ASTM.
                               E-43

-------
Date:
           DRY GAS  THERMOMETER CALIBRATION DATA  SULLT
Thermometer No. :
Ambient temperature:    x>2-  °T  Barometric pressure:

Calibrator; /? /I <-rr\ s f- r^<-<-    Reference:

Reference
point
No.
1
2
3


Source, *
2
I
3
Reference
thermometer
temperature,
°F***
72. &
32.7
tfo. o
Thermometer

temperature, Difference,
Op **
V/ ' °
?0 c.3
I £ £• V«- o
                         Figure E-9 (continued)
  *Source:  1)  Ice  bath
            2)  Ambient
            3)  Furnace  set at approximately  110°r

 **Difference must  be  less than or equal to  +5°F.

***Reference thermometer must be ASTM.
                             E-44

-------
            DRY  GAS  THERMOMETLR CALIBRATION DATA S11LLT
Date:
O
Thermometer No. :
Ambient temperature:

Calibrator :  /?     -
        T  barometric pressure:

          Reference:     A '

Reference
point
No.
1
2
3
l
Rcfercr.ce

Source, *
2
1
Thermometer
thermometer 1
temperature ,
op***
7?&
52.1
i
3 j ) | £, . o
temperature, Difference,
"7 ' 2~ &•&
32 0: 7
\(3 ; 3.C
                         Figure E-9 (continued)
  *Source:  1) ice bath
            2) Ambient
            3) Furnace set at  approximately HOT

 **Difference must be less than or  equal  to +5T.

***Reference thermometer must  be ASTM.
                            E-45

-------
           DRY GAS  THERMOMETER CALIBRATION DATA  SHEET
Date:
Ambient temperature:

Calibrator:  (3.  A ri^.
  Thermometer No. ;  f- B~3    Oo-H-g-^"

'T  barometric pressure: ^9 3'ff  " H;

                      -2. 
32.7 JO *,7
)H. 0
1
/ ' ~-' \ ^ *
                         Figure E-9 (continued)
  *Source:  1)  Ice  bath
            2)  Ambient
            3)  Furnace  set at approximately  110°F

 **Difference must  be  less than or equal to  +5°F.

***Reference thermometer must be ASTM.
                               E-46

-------
           DRY  GAS  THERMOMETER CALIBRATION DATA SHLLT
                               Thermometer No . :
Date:	    	                   	
              ^7   7
Ambient temperature:   ~7£   °r  Barometric pressure:

Calibrator: /?. /\ ff^ * T,- r ._    Reference:
                                                               " l)<

Reference
point
No.
1
2
3
1 i 1
Reference Thermometer

Source, *
2
1
3
thermometer i
temperature ,
op***
~7Z.*
32 7
1'. >- 0
temperature, Difference,
Op **
"7 9 & c'
f £—
72 °- 7
i"/ , /• "
                         Figure E-9  (continued)
  *Source:  1) Ice bath
            2) Ambient
            3) Furnace set  at  approximately 110°r

 **Difference must be less  than  or equal to +5°F.

***Reference thermometer must  be ASTM.
                              E-47

-------
Date:
DRY GAS THERMOMETER CALIBRATION  DATA SHLET


                   Thermometer No.:   F & - i.
              /Y
Ambient temperature:   *?2-
Calibrator:
             •9
                   '  Barometric  pressure ;

                   Reference :
                                                                 H<;

Reference
point
No.
1
2
3


Source , *
2
1
3
Reference
thermometer
temperature,
op* * *
72.o
37.1
1 f *"*. ^
Thermometer

temperature, Difference,
op * *
72 i-v
1Z 0,7
fit. : *.o
                          Figure E-9 (continued)
  *Source:  1) Ice bath
            2) Ambient
            3) Furnace set at  approximately 110°F

 **Difference must be less than  or  equal to +5°F.

***Reference thermometer must  be ASTM.
                                E-48

-------
           DRY GAS THERMOMETER  CALIBRATION DATA SHEET
Date:
  Thermometer No.:
Ambient temperature:

Calibrator;
°F  Barometric pressure;

  Reference:  A^T/* - 3
                                                              " Hg

Reference
point
No.
1
2
3


Source, *
2
1
3
Reference
thermometer
temperature,
op***
?S
3 t
/£0
Thermometer

temperature,
OF
•7S
3S
fZC>


Difference,
**
©,o
2, a
o, O
                         Figure E-9 (continued)
  •Source:  1) Ice bath
            2) Ambient
            3) Furnace set at approximately  110°F

 **Difference must be less than or equal  to  +5°F.

***Reference thermometer must be ASTM.
                              E-49

-------
           DRY GAS THERMOMETER  CALIBRATION DATA SHEET
Date:
                               Thermometer No.:
Ambient temperature:
   £
Calibrator: /?,
°F  Barometric pressure:

  Reference:   y4.S T~S^ ~
                                                              " Hg

Reference
point
No.
1
2
3


Source, *
2
1
3
Reference
thermometer
temperature ,
ep***
?/
££
/Zo
Thermometer

temperature,
Op
•>/
*y
(20


Difference,
**
c^.-o
2.^>
o.o
                          Figure E-9 (continued)
  *Source:  1) Ice bath
            2) Ambient
            3) Furnace set  at  approximately 110°F

 **Difference must be less  than  or equal to +5CF.

***Reference thermometer must  be ASTM.
                                  E-50

-------
                    TRIP  BALANCE ACCURACY LOG
Trip bal.
 number
Date
Calibrator
 Ref .
weight
 Weight
observed
Difference
                           £
                               *
  n*
                                      00
            Figure E-10.  Trip balance accuracy loq.
                          E-51

-------
Pre-test
                          BAROMETER  CALIBRATION  LOG
Barometer
Number
Project
Number
2-2^
ffg^T
?.*n
£114
225^
J-/77
^37
^C7&
&7
352r-/7




Barometer
Reading
Reference
Barometer
Reading
Difference*

2 L

In. -$z-
o- <=o










Post-test
                   /
Barometer
Reading
Reference
Barometer
Reading
Difference**
2 \ :'«-'
• 5 t—t ••» jr •
s f *+ c. *
t> cO
JIO.-3--
3'/ 3^
c^ ^<>
^^ v^
oo ^!
C>.^












*  Barometer is adjusted so that difference does  not exceed 0.1"Hg.
** Barometer is not adjusted,  difference must not exceed 0.2"Hg.


                     Figure E-ll.  Barometer calibration log.
                                     E-52

-------
       APPENDIX F




QUALITY ASSURANCE SUMMARY
           F-l

-------

-------
                    QUALITY ASSURANCE SUMMARY

     The following sununary addresses factors that ultimately are
used to ensure data quality and accuracy for any given emission
test project.

PROJECT ORGANIZATION AND RESPONSIBILITES
     The project organization and responsibilities are generally
defined in the test plan.  Specific responsibilities for this
field test are shown in the list of project participants in
Appendix G.

QA OBJECTIVE
     The QA objective of the data collection was to provide infor-
mation to be used by the State of Iowa DEQ in writing a State
Implementation Plan (SIP) for lead acid battery plants.  There-
fore all procedures used to collect and analyze emissions samples
followed EPA reference methods where applicable.  No attempt was
made to determine precisions, because the precision of these
reference methods had previously been determined.  Modifications
to Methods 5 and 12 were necessary in order to perform emission
tests at the Carter-Day baghouse outlet site.  The reason for the
modification of the Methods 5 and 12 procedures was that the loca-
tion of the sampling ports were such that a flexible line had
                               F-3

-------
to be used to connect the filter holder to the first impinger.
The precision of the modified method was not determined because
such determination was not included in the scope of the project.
The completeness of the data was the same as required for a per-
formance test as defined in 40 CFR 60, Section 60.8.  The emis-
sion results were to be representative of normal operations.  The
data and results were presented in several units to allow for
comparability with data from all other organizations wishing to
access the data summary.
DATA REDUCTION, VALIDATION, AND REPORTING
     Data reduction and reporting have been shown to be great
potential sources of system error.  Most of PEDCo's test method
calculations are performed by a validated computer program  to
minimize error.  The field data sheets are also set up on a
standard computer card to allow accurate input of data into  the
computer by individuals unfamiliar with testing procedures.   The
data printout is then validated by comparison with the field and
analytical data sheets.  In addition, hand calculation checks  are
generally made to validate the computer output.  Other data
validations are made whenever possible.  The  reporting format
provides  efficient  and  effective  review of all  data  and  results.

 PERFORMANCE AND SYSTEM AUDITS AND FREQUENCY
      When feasible, PEDCo  performs both performance and  system
 audits.   A performance audit for  accuracy was performed  in the
 field on all  dry gas meter systems using critical  orifices.  An
 Iowa State DEQ representative was onsite and monitored testing
 procedures.
                              F-4

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SPECIFIC ROUTINE PROCEDURES USED TO ASSESS DATA PRECISION,
ACCURACY, AND COMPLETENESS

     No attempt was made to assess data precision, which had

been reported elsewhere or else was not in the scope of the

report.  Precision results for EPA reference methods are sum-

marized in "The EPA Program for the Standardization of Stationary

Source Emission Test Methodology, A Review," EPA-600/4-76-044.

PEDCo has been a collaborator in several of the EPA programs to

determine method precision.  In all cases of final data summary

reporting, PEDCo was within two standard deviations of the

method precision.  Based on the  quality and experience of the

test team used in this test series, all data summaries are likely

to be within one standard deviation of the documented precision,

as determined for a single run for each specific reference

meter.  The accuracy audit procedure used for the dry gas meter

is the standardized written procedure used by the EPA Quality

Assurance Division program.  The procedure for determining com-

pleteness of data is the same as the specified in 40 CFR 60,

Section 60.8.


INTERNAL QUALITY CONTROL CHECKS

     Several internal quality control checks are usually made

for each test.  The majority of these checks usually deal with

the field sample analysis.  Filter blanks were returned to the

laboratory for gravimetric analysis.  This control checked the

quality of both the initial and the final weighing.
                               F-5

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CORRECTIVE ACTION
     PEDCo has two methods for corrective action.   The first is
the use of control limits.  Examples of control limits are audit
sample results, control sample results, and calibration results.
When any of these limits show that data are of questionable
integrity, then the procedure is repeated, additional data are
collected, or the data are rejected.  The second method is the
use of red tags.  Whenever any piece of equipment is suspected of
producing unacceptable data, the entire apparatus or malfunc-
tioning component is replaced and a red tag is placed on the
item.  That piece of equipment is then rejected until its ability
to perform its function properly is verified by the proper
individuals.  The use of control limits and red tags reduces the
amount of unacceptable data and provides a system to track and
correct unacceptable items and procedures.

PREVENTIVE MAINTENANCE PROCEDURES AND  SCHEDULES
     PEDCo has a comprehensive preventive maintenance program.
Many major components of test equipment have pretest checklists.
These checklists ensure that all functions are checked  and  that
action is taken to repair or replace any part  likely  to malfunc-
tion.  These checks are made before every  field test  series;
however, only the control console  (meter box) checks are re-
corded.  Although the preventive maintenance program and schedule
are  not in writing, PEDCo's commitment of three full-time, ex-
perienced personnel for equipment construction, preparation,
                                P-6

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calibration, and maintenance has resulted in a program based on



experience and skill that cannot be matched by a program based on



written guidelines.






QUALITY ASSURANCE REPORTS TO MANAGEMENT



     The standard quality assurance procedures used in this test



program generate sufficient documentation to 'indicate the quality



of data.  All evidence of the execution of the quality assurance



guidelines is reviewed by management.
                               F-7

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             APPENDIX G




PROJECT PARTICIPANTS AND ACTIVITY LOG
                  G-l

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CN
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TABLE G-l.   PROJECT PARTICIPANTS
Name
M. Phillips
J. Prohaska
J. Thomas
D. Fitzgerald
P. Rei nermann
S. How i son
D. Durst
D. Phelps
L. Thomas
Affil iation
PEDCo
PEDCo
PEDCo
PEDCo
PEDCo
PEDCo
EPA
Iowa, DEQ
Prestol ite
Activities
Coordinate test activities, liaison with
plant, site preparation, monitored process
operation
Performed Methods 5 and 12 runs at the
Entoleter scrubber, Barton Oxide process
baghouses and baghouse No. 1
Assisted in tests at the Entoleter scrubber
Barton Oxide process baghouses, and bag-
house No. 2
Performed Methods 5 and 12 runs at the
Carter-Day baghouse and baghouse No. 3
Assisted in tests at the Carter-Day bag-
house and performed Methods 5 and 12 runs
at baghouse No. 2
Performed sample recovery for Methods 5 and
12 runs. Assisted in tests at baghouse
Nos. 2 and 3
Project officer, monitored test performance
Monitored testing procedures
Plant contact, general assistance
               G-3

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TABLE 6-2.   FIELD SAMPLING  LOG
Day
Saturday

Sunday

Monday




Tuesday


Wednesday



Thursday


Friday



Saturday
Date,
June 1981
6

7

8




9


10



11


12



13
Activity
Transported equipment to site (1 man); traveled to
site (4 men).
Set up equipment; took Method 1 measurements (5 men);
traveled to site (1 man).
Took Method 2 measurements at all sites; prepared
sampling trains; conducted two Method 12 runs at the
Barton Oxide baghouse; conducted one Method 12 run at
the Entoleter scrubber; conducted one Method 12 and
one Method 5 run at the Carter-Day baghouse.
Conducted one Method 12 and one Method 5 run at the
Barton Oxide process baghouse and Entoleter scrubber;
conducted one method 12 run at baghouse No. 3.
Conducted one Method 12 run at the Entoleter scrubber
and Carter-Day baghouse; conducted two Method 12 runs
at baghouse No. 3; conducted two Method 12 runs and
one Method 5 run at baghouse No. 1.
Conducted one Method 12 run at baghouse No. 1; con-
ducted one Method 12 and one Method 5 run at baghouse
No. 3; conducted two Method 12 runs at baghouse No. 2
Conducted one Method 12 and one Method 5 run at bag-
house No. 2; packed equipment and left site; returned
to base (5 men); departed with equipment and samples
(1 man).
Returned to base with equipment and samples (1 man).
               G-4

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TECHNICAL REPORT DATA
(Please read Instructions on the reverse before completing)
1. REPORT NO.
EPA 907/9-81-008
2.
4. TITLE AND SUBTITLE
Emission Test Report-Prestolite Lead Acid Battery
Plant, Manchester, Iowa
7. AUTHOR(S)
9. PERFORMING ORGANIZATION NAME Ah
PEDCo Environmental, Ii
11499 Chester Road
Cincinnati, Ohio 4524£
JD ADDRESS
1C.
12. SPONSORING AGENCY NAME AND ADDRESS
Environmental Protection Agency, Region VII
Air and Radiation Branch
324 East llth Street
Kansas City, Missouri 64106
3. RECIPIENT'S ACCESSION-NO.
5. REPORT DATE
October 1981
6. PERFORMING ORGANIZATION CODE
8. PERFORMING ORGANIZATION REPORT NO.
PN 3525-17
10. PROGRAM ELEMENT NO.
11. CONTRACT/GRANT NO.
68-02-3512
Work Assignment No. 17 '
13. TYPE OF REPORT AND PERIOD COVERED
Final
14. SPONSORING AGENCY CODE
15. SUPPLEMENTARY NOTES
16. ABSTRACT
This document is a final report on stack testing conducted at the Prestolite
lead acid battery plant. The purpose of the test was to provide lead and
particulate emissions data for the major sources of lead at the plant. Lead
sampling and analytical procedures followed those described in EPA proposed
method 12 in the Federal Register of January 14, 1980 (45 FR 2790). The
testing adhered to acceptable quality assurance procedures which are docu-
mented in the report.
The plant was operating at a production rate of approximately 3600 batteries
per day when tested. The maximum output for the plant is 4100 batteries per
day. Pure lead is obtained from an outside source and lead oxide is manu-
factured by the Barton process. The major operations employed at the plant
are lead oxide production, grid casting, paste mixing, battery assembly
(the three-process operation) and formation (wet and dry). The report lists
the lead and particulate emission rates from each emission point tested.
Based upon the test results, the maximum lead emissions from the plant are
1.54 tons per year and the average lead emission rate is 1.13 tons per year.
17.
a. DESCRIPTORS
Air Pollution
Particles
Lead
Battery Plant
18. DISTRIBUTION STATEMENT
Unlimited
KEY WORDS AND DOCUMENT ANALYSIS
b. IDENTIFIERS/OPEN ENDED TERMS
Source Test
Method 12
Method 5
19. SECURITY CLASS (This Report)
Unclassified
20. SECURITY CLASS (This page)
Unclassified
EPA Form 2220-1 (9-73)

c. cos AT I Field/Group

21. NO. OF PAGES
438
22. PRICE


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