<\\\\~
Fr Way
January 4, 1985
Part V\
Environmental
Protection Agency
40 CFR Part 136
Guidelines Establishing Test Procedures
for Hie Analysis of Pollutants Under the
Clean Water Act; Final £ule and Interim
Final Rule and Proposed Rule;
Corrections
02
HEADQUARTERS LIBRARY
ENVIRONMENTAL PROTECTION AGENCY
WASHINGTON, D.C. 20460
CD
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600
Federal Register / Vol. 50. No. 3 / Friday, January 4,1985 / Rules and Regulations
ENVIRONMENTAL PROTECTION
AGENCY
40 CFR Part 136
IFRI.-2737-4J
Guidelines Establishing Test
Procedures for the Analysis of
Pollutants Under the Clean Water Act;
Correction and Extension of Comment
Period on Interim Final Rule
t
AGENCY: Environmental Protection
Agency (EPA).
ACTION: Interim final and final rule:
corrections and extension of the
comment period on the Interim Final
_p.qrtipn of the rule.
SUMMARY: EPA is correcting the
Preamble, Final and Interim Final
Regulations and Appendices to
regulations establishing Guidelines for
Test Procedures for the Analysis of
Pollutants Under the Clean Water Act
which was published in the Federal
Register of October 26.1984,49 FR
43234. In response to requests to allow
for a longer time period to review the
supporting record. EPA is extending the
comment period by sixty days.
FOR FURTHER INFORMATION CONTACT:
Dr. Robert Medz. Environmental ''•
_Mcnitoring:Systems Division. Office of
Research and Development (RD-680),
U.S. Environmental Protection Agency.
401 M Street SW.. Washington. D.C.
20460, Telephone Number (202) 382-
5792.
DATE: Comments on the Interim Final
Rule must be submitted on or before
February 25,1985.
SUPPLEMENTARY INFORMATION: In FR
Doc. 84-26189 appearing at page 43234
in the Federal Register of Friday,
October 26.1984. EPA published a
preamble, a Final and interim Final
Regulation and Appendices establishing
guidelines for Test Procedures for the
• Analysis of Pollutants Under the Clean
Water Act. The Preamble and
Appendices contained typographical
and other errors which EPA is today
correcting. In addition. EPA is correcting
the citations of several supporting
documents to indicate that they are
available through the National
Technical Information Service (NTIS).
In response to several requests for an
extension of the comment period, the
EPA is extending the end of the
comment period by sixty days from
December 26.1984 to February 25.1985.
EPA has discovered that several
approved test procedures were
inadvertently omitted. The following
tables and paragraphs indicate the
omitted test procedures, and the >
references from which they are
incorporated. Incorporation by reference
of these references has been approved
as of the effective dates published in 49
FR 43234 by the Director of the Federal
Register.
Table/parameter
Reference Ifom when incorporated
PA. Conform |l«cai) >n
presence ol
cWonne
MF.—909C
124...
-B-0050-77....
IB. Hardness. EOTA
Tiiraton—page 556.
Hydrogen ion. pH.
Eieetromeine—
page 547
Manganese.
penodate—page
227.
Nitrate
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Pectoral Register / VoL SO. No. » / Friday, January 4.1985 J Rules and Regulations
891
f
I
the October 28.1964 printing to the
correct Value of "7-days".
EPA is correcting these errors and
other typographical eurors an the Gnal
regulation.
Dated: Decombnr it. 1984.
Bernard D. Goldstein.
Assistant Administrator, -Offioe|g« •«•.. j
P»M »32—
4g* •««.-.- j
sumJMi :
mMhoitt 1
i5m«dL . '
90BC ;.
9WC
•SMC
<
ASTM ,
•
USGS>
B-OCBO-77.
B^O05O-T7.
ntil.Piot«
Agmcy.
'Tlw nwttxM UMd mMl IM »p«cified when mulB «r« rwxmeA
'•'MiooOioloaical Meinods (or Montonng in* Environmwit. Water md WttW, 1978". EPA-600/S-78-01T. U & E
'G(«eson. P.E.. «f «. "Mtinods for Coiiecoon ana Arwlysii of Aqu*oc Boloffcal *nd MJcraeiolovcal SunvlM.
Sook S. Chanter M, Laboniory Arulysa. 1977. .. „
0 45 urn mwriran* W«r or ollw pom «• cwtfwd by M m«nu(«cturer to fully main orginunt to bt oullivitML and fr*t o< «itractabl«i orNcri coJd inMrtom wOh^llMir grown and
>pinant • . . .» . — r
*-Sino* BK mfrnarirw ffltw tecfimju* usually yMdi low and variable raeovtry from oMoria*t«t muttMaura. tf» MfN mwiKxJ witTM r*ouir«t 10 nnotMijmy commnma.
1*
14. On page 43251. Table IB,
parameter 6. Arsenic, •change -the
method descriptor "Hydride" to "AA
(gaseous hydride}".
15. On .page -43252. Tattle IB,
parameter 17, Chlorine, delete the first
three methods and fheTespective
references and replace with •fbe
following methods and references to
read:
C1. 33QJ1 ^MC '.DI2S3-
jgpjft 40BA 1>12£B-
76
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692
Federal Register / Vol. 50. No. 3 / Friday, January 4.1985 / Rules and Regulations
Methods. 15th edition", incorporate the
reference citation "32SB".
26. On page 43254. Table IB.
parameter 65, Sulfate, change the
method descriptor "Automated
methyithymol blue" to "Automated
Colorimetric (barium chloroanilate)" and
change the incorporated reference under
EPA from "375.2" to "375.1": delete the
reference "1-2822-78" under the USGS
column.
27. On page 43254. Table IB.
parameter 74. Vanadium, opposite the
method descriptor "Colorimetric (Gallic •
acid)" under the reference column
heading "Standard Methods. 15th
edition", incorporate the reference
citation "327B".
28. On page 43254. Table IB.
parameter 75. Zinc, insert a line between
the method descriptor "Inductively
coupled plasma" and "Colorimetric
(Zincon)". and insert the method
descriptor "Colorimetric (Dithizone)":
opposite the method descriptor
"Colorimetric (Dithizone)" under the
reference column heading "Standard
Methods. 15th edition" incorporate the
reference citation "328C".
29. On page 43255. Table IB. footnote
7. line 2. change "traditional CBOD»" to
read "traditional BOD*".
30. On page 43255. Table IB Notes.
add a new footnote to read: *• The
approved method is that cited in the
"Standard Methods for the Examination
of Water and Wastewater". 14th edition,
1976.
31. On page 43255. Table 1C.
parameter 11, change "(ghi)" to read
"(g.h.i)".
32. On page 43255. Table 1C.
parameter 13, change "Chloride" to
"chloride". —- ——~
33. On page 43255, Table 1C.
parameter 14, change "Butyl Phthalate"
to "butyl phthalate".
34. On page 43256. Table 1C.
parameter 66. change "Chloride" to
"chloride".
35. On page 432S6. Table 1C
parameter 67. change "2-Methyl-4.6-
Dinitrophenol" to "2-Methyl-4.6-
dinitrophenol".
35. On page 43256. Table 1C.
parameter 68 under the column labeled
HPLC. delete the "......" and add "610".
37. On page 43256. Table 1C.
parameter 75, change "2,2-oxybis(1-
chloropropane)" to "2.2'-Oxybis(l-
chloropropane)".
38. On page 43256, Table iC.
parameter 97, change "Chloride" to
"chloride".
39. On page 43257. Table ID.^the,
-method'descriptor follbwihg'parameter
42 "GC/MS 625" should be moved up
one line to accompany parameter 41 and
read as follows:
41. moucMor «po«Wt...~..-~ .- - _..._ . —.
GC
GC/MS
EOS
• Sis
509*
D308S
Note 3 p. 7 Nott 4
p. 3ft Not* 6. p.
S73.
40. On page 43257. Table ID. parameter 42. should read:
a l*Klr«i ,
fftj
|«OM 4. p. 30; Not* 6.
(HS73.
41. On page 43257. Table ID.
parameter 56. change "Prometon" to
"Prometron".
42. On page 43258. in column 2 of the
Table, of References, Sources and Costs.
add parameters 34,38 immediately
before and 52 immediately after
parameter 48 to the list of parameters on
line 7 which are found in Table IB and
which are incorporated by reference
from the 14th edition of "Standard
Methods for the Examination of Water
and Wastewater."
43. On page 43258, in column Z of the
Table of References. Sources, and Costs.
add parameter 2 between parameters 1
and 3 on line 12. which are found in
Table LA and which are incorporated by
reference from the USGS Methods for
Collection and Analysis of Aquatic.
Biological, and Microbiological Samples.
44. On page 43258. Table of
References. Sources, and Costs, move
line 11 "1B-EPA" in column 1. and line
13 "1-13.15-48. 50-75" in column 2
down so they are opposite the EPA
reference on line 24 of column 3. entitled
"Methods for Chemical Analysis of
Water and Wastes",
45. On page 43259, in column 2 of the
Table of References, Sources, and Costs,
add parameters 27 and 28 between
parameters 22 and 30 to the list of
parameters on line 3 which are found in
Table IB and which are incorporated by
reference from "Official Methods of
Analysis of the Association of Official
Analytical Chemists," 13th Edition, i960.
46. On page 43260, Table II. under the
column heading "Maximum holding
time" for parameter 54. Residue.
Filterable, change "48 hours" to "7
days".
47. On page 43262, column 2. section
6.3.1, change "Barnebey" to "Bamabey".
48. On page 43265. column 3. change
reference 9 to read:
9. "EPA Method Study 24. Method 601—
Purgeable Halocarbona by the Purge and
Trap Method." EPA 600/+-94-O64. National
Technical Information Service. PB84-212448.
Springfield. Virginia 22161. July 1984.
49. On page 43268, delete the
handwritten number "-170-" from the
bottom of the page.
50. On page 43275. column 1. section
8.7, line 7, change "recommended to
encompass" to "that encompass".
51. On page 43276. column 1, change
reference 2 to read:
2. Lichlenberg. J.J. "Determining Volatile
Organics at Microgram-per-Litre-Levels by
Gas Chromatography," journal American
Water Works Association. 66. 739 (1974).
52. On page 43276. column 3, change
reference 9 to read:
9. "EPA Method Study 25. Method 602.
Purgeable Aromatics," EPA 600/4-84-042.
National Technical Information Service,
PB84-196682. Springfield, Virginia 22161, May
1984.
53. On page 43283, column 2, section
8.2.5. line 2, delete "either".
54. On page 43284. column 3. change
reference 3 to read:
3. "Evaluate Te»i Procedures for Acrolein
and Acrylonitrile." Special letter report for
EPA Project 4719-A. U.S. Environmental
.J5--
-------
ftegjuter / Vai sa N«. 3 / Friday. January 4.1985 / Rrfea and ttegulatmia
693
Protection Agency. Enuironmantal Monitoring
and Support Laboratory. Cincinnati. Ohio
45268. 277une tBTB.
55. On page 43284. column 3. change
reference • to read:
9. "Evaluation of Method 80S (Modified)."
EPA-680/4-84-ABC National Technical
information Service. PB84-. Springfield.
Virginia 22161. Nov. 1984.
58. On page 48298, oolinrmZ Motion
10.2.2. line 3, change ">epor'"tO
. "excess"-.
57. On page 43294, cufhimn A change
reference 2 to read:
2. *'.DalBnmn8tin«l Technical Information
Service, PB81-232167, Springfield, Virginia
22161, ju|y 19SL -
62. On |i*ge-4930g, column 3, aft ithe
endBI2 —
Chtorinated Uydncatbenfl," EPA .800/*-«-
039. National Technical Jnfionnation-.Senrica,
PB64-187772. Springfieia. Viipnia
1984. ' , .......
A2.OnipHge-4aaJa.
Refenancei to aank
2. 'TJelEnrrinrton oTTCBBrhi'hiflustTiai
and Municipal WaslewateTs,-';EPA'680/4-S2-
028. National Technical WfonnaticmSeTvice,
PB82-I96a82.-Snringrield. Viigjnia 32161.. ftpr.
198Z
83.*Onjiage 43373, column 3, dhange
Reference 35 to.iea& *
IS. '0>AJ4eihodShidy^&
800/4-84-037. NaBnnalT«dhnical4nIonnatioji
Service, PBa4-188879, Springfield. Virginia
22181,1Hayl88a.
84.On.page 43S3J3..colunin.3. Table 1,
delete comma after 8 toTead: 2,3, 7.8-
TCDD.
85. On page-43378,iOdhnnii2.
Reference 11, peplaae-line4 by: "May 14,
1980.".
86. On -pege-4B87B, -cdlumn-Z, tdhange
Reference 12 to read: • ••
12, "EPA Memoa*Study ZB&PCMe&aa
824— Purgeables,"£RA 60Q/4-WI-OM.
NatiDnaTTechnieannfonnafi on 'Service.
PB84-20991S, SpringTiel4tVirgniia.Z21Bl,'Iune
1984. .
87. On page-43385, .colunm X.aeclion
1.3. line 2, after the word "method" add
two references to read as follows:
"method*1***,
88. On page 43385. column 4, section
2J1. line 03. -delete the watds "either
external >or".
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694
Federal Register / Vol. 50. No. 3 / Friday. January 4.1985 / Rules and Regulations
89. On page 43388. column 3, section
7.2. line 13. change "masses" to "m/z
quantities".
90. On page 43389. column Z, section
13.3. lines t and 2. delete the phrase. "If
the internal standard calibration
procedure is being used", and use the
remainder of the sentence as the first
sentence of section 13.3 to read as
follows: "The internal standard must be
added to the sample extract and mixed
thoroughly immediately before it is
injected into the instrument."
91. On pay 43390. column 2. change
date at the end of Reference 13 to "May
14,1980.".
92. On page 43390. column 2. change
Reference 14 to read:
». "EPA Method Study 30. Method 625.
Base/Neutrals. Acids, and Pesticides," EPA
600/4-84-053, National Technical Information
Service. PB84-206S72. Springfield. Virginia
22181, June 1984.
93. On page 43390, column 2, Table 1,
change "Bis(2-chloroethy!)-ether" to
"Bis(2-crJoroethyl) ether".
^ jj4^Oj>.pjige^MM.jnpJujnjn^2/rable 1.
"change "Bis(2-chloroisopropyl) ether" to
"Bis(2-chloroisopropy!) ether •" and add
a footnote to Table 1 to read: "• The
proper chemical name is 2,2'-oxybis(l-
chloropropane)".
95. On page 43390. Table 4, add a new
footnote "•" after the parameter "Bis(2-
chloroisopropyl) ether" to read: "Bis{2-
chloroisopropyl) ether •".
96. On page 43391, Table 4, change
"Diethylphthalate" to "Biethyl
phthalate".
97. On page 43391, Table 4, line 21,
under column heading "Secondary"
change the number "338" to "339".
98. On page 43391. Table 4. line 42,
change "Indeno (1, 2,3-c; d) pyrene" to
"Indeno(l. 2,3-cd) pyrene".
99. On page 43391. Table 4, change
footnote designations "a" after
parameters on lines 8.10.12. 21, 26,27.
29, and 45 to footnote "b".
100. On page 43391. Table 4. change
footnote designations "b" after
parameters of lines 46*-54 to footnote
"c".
101. On page 43391. Table 4, add a
new footnote "a" to read: "a The proper
chemical name is 2.2'-bisoxy(l-
chloropropane}".
10Z On page 43391. Table 4. change
footnote designation "•" to "*".
103. On page 43391. Table 4, change
footnote designation "*" to "*" and
merge the three lines of footnote text to
read:
"* These compounds ace mixtures of
various isomers (See figures 2 through 12).
Column conditions: Supelcoport (100/120
mosh) coated with 3% SP-2250 packed in a 1.8
m long x Z mm ID glass column with helium
carrier gas at 30 mL/min flow rale. Column
temperature held isothermal at 50 °C for 4
min. then programmed at 8 °C/min to 270 °C
and held for 30 min."
104. On page 43392. Table 6. line 13.
change "Bis(2-chioroethyl)ether" to
"Bis(2-chloroethyl) ether".
* 105. On page 43392, Table 6, line 15.
change "Bis(2-chloroisopropyl)ether" to
"Bis(2-chloroisopropyl) ether •".
106. On page 43392. Table 6, line 16.-
change "Bis(2-ethylhexyl)-phthalate" to
"Bis(2-ethylhexyl) phthalate".
107. On page 43392. Table 6. line 35.
change "Oi-n-octylphthalate" to "Di-n-
octyl phthalate".
108. On page 43392. Table 6, at the
bottom of the table after the NOTE, add
a new footnote "a" to read:
"The proper chemical name is
2,2'oxybis(l-chloropropane)".
109. On page 43392. Table 7. line 13.
change "Bis(2-chloroethyl)-ether" to
"Bis(2-chloroethyl) ether".
110. On page 43393, Table 7. line 2.
change "Bis(2-chloroisopropyl]-ether" to
"Bis(2-chloroisopropyl) ether •."
111. On page 43393, Table 7. line 3.
change "Bis(2-ethylhexyl)-phthalate" to
"Bis(2-ethylhexyt) phthalate".
112. On page 43393. Tab!e<7, line 22.
change "Di-n-octylphthalate" to "Di-n-
octyl phthalate".
113. On page 43393. Table 7. add a
new footnote "a" to read:
"• the proper chemical name is
2,2'oxybis(l-chloropropane)".
114. On page 43393, Table 8. lines 10
and 11, change the parameters "1- '
Fluoronaphthylene" and "2-
Fluoronaphthylene" to "1-
Fluoronaphthalene" and "2-
Fluoronaphthalene".
115. On page 43407, column 1, section
2.3. line 5. delete the words "or
external".
116. On page 43408. column 1. section
6.5.1.2, line 5, change "approx" lo
"approximately".
117. On page 43408, column 3, section
6.7.4, line 1. change "Othe" to "Other".
118. On page 43409. column 1. section
7.4, line 8, delete the words "or
external".
119. On page 43409. column 1. section
7.4.3. line 3. change "figure 5" to "figure
6".
120. On page 43410. column 3. section
10.6. delete the sentence or. lints 15-17
which reads: An example of
the . . . shown in figure 5.
121. On page 43412. column 1. change
Reference 9 to read:
9. "EPA Method Study 29 El'A
624— Purgeabies." EPA 600/+-W-UM.
National Technical lnfarm;inon S«rm,tv
PB84-209915. Springfield. Vinjmn 2:181. |unr
1984.
122. On page 43412. column 1. Table 1.
line 16. for 1.2-dichloroethane. change
the Storet number from '"32103" to
"34536".
123. On page 43412. column 3, Table 3.
insert a new mass 175.and intensity
required and change limits for mass 176
to read:
174
175 5 to 9 percent of mass 174
176 95 to 101 percent of mass 174
124. On page 43416. column 1, section
2.3. line 5, delete the words "or
external".
125. On page 43416, column 2. section
4.2. line 4, insert "benzidine" between
the colon and "benzo(a)anthracene".
126. On page 43416. column 2. section
4.2. line 7, change "B-naphthylamine" to
"0-naphtylamine".
127. On page 43416, column 3.- section
5.5, line 2, change "(q" to "±".
128. On page 43417. column 1, section
6.7, line 15. change "ug/mL" to '>g/mL".
129. On page 43417, column 2. section
6.13. line 9, change "lOuL" to "10 u.L".
130. On page 43417, column 3, section^,
7.3.1. lines 4 and 5, change "ug/mL" to
'>g/mL".
131. On page 43417, column 3. section
7.4, line B, delete the words "or
external".
132. On page 43422. Table 1. line 20.
change "a-picoline (Synfuel)-" to "a-
Picoline (Synfuel)".
133. On page 43422. Table 3. line 30
(EGD 234), change "2,4-dtmethyl phenol"
to "2,4-dimethyl phenol-d3".
134. On page 43424. Table 4, after the -
. Temperature program footnote, change
": 30-250 *C" to ": 8 'C/min to 250 'C".
135. On page 43424, Table 5, line 1 (m/
z 51), change "30-80" to "30-60"; and at
line 4 (m/z 127), change "30-60" to "40-
60".
136. On page 43424, Table 5, add a
new specification for m/z 365 and
change the intensity required for mass
441 to read:
275
365 greater than 1 percent of mass 198
441 present and less than mass 443
Appendix B to Part 136—(Corrected)
137. On page 43430, section 5. column
3, first line under "where:"
delete the second "=" to read:
where:
Xi: i = l to n, are the analytical results in
138. On page 43430, section 7.(a), line
4 change the phrase "spike in the matrix
at the" to "spike the matrix at this".
139. On page 43430. section 7.{b). line
6. reverse the subscript and superscript.
of "S" from "SV to "SV- and changeV*'
"others" to "other".
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Federal Register / Vol. 50. No. 3 / Friday. January 4.1985 / Rules and Regulations
695
140. On page 43431, colufnri i Tables
of Student's t Values, under column
heading "Degrees of freedom", line 6.
change "10" to "15".
Appendix C to Part 136—[Corrected]
141. On page 43433. column 3. section
7.8.2. lines IB to 19. delete the last
sentence.
. . . report. May 14.1980.
[FR Doc. 85-234 Filed 1-3-65:8:45 am|
BILLING COPE I9CO-3MI
40 CFR Part 136
[FRL-263&-6!
Guidelines Establishing Test
Procedures for the Analysis ol
Pollutants Under the Clean Water Act
'Correction"
In FR Doc. 84-26189 beginning on page
43234 in the issue of Friday. October 26.
1984. make the following corrections:
1. On page 43237, column 1. line 33.
change "as" to "a".
2. On page 43239. column 1, last line.
change 'Table" to "Tables".
3. On page 43242. column 2. EXHIBIT
1. the heading over the last and the next
to last columns should be changed to
read:
Number of Test Criteria Failures
Start-up» • On-going * '
4. On page 43243, EXHIBIT 2, last
column, line 7, change "HCl" to "HC1".
7. On page 43250. column 2. first
paragraph line 2. change "January 22" to
"January 24".
$136.3 [Corrected]
8. On page 43251. Table IB heading.
change "IB" to "IB".
9. On page 43252. Table IB heading.
change "IB" to "IB".
10. On page 43253. Table (B heading.
change "IB" to "IB".
11. On page 43253. Table IB.
parameter 34. change "Maganese" to
"Manganese".
12. On page 43254. Table 18 heading.
change "IB" to "IB".
13. On page 43255, Table 1C.
parameter 10, change
"Benzo(b)fluroanthene" to
"Benzo (b] fiuora nt hene".
14. On page 43257. Table ID.
parameter 16. change "Chloroprapham"
to "Chloropropham".
APPENDIX A TO PART 136—
{Corrected]
15. On page 43261. column 1. table in
section 1.1. change the CAS No. after
trans-1.3-Dichloropropene to "10061-02-
6".
16. On page 43261. column 1. table in
section 1.1. change "1.1,1-
Tetrachloroethane" and "1,1.2-
Tetrachloroethane" to "1.1.1-
Trichloroethane" and "1.1.2-
Trichloroethane".
17. On page 43275. column 3. section
12.2. line 3, change "1000 X MDL" to
"100 x MDL,"
18. On pages 43278. 43279. and 43280,
delete handwritten page numbers "-208-
". "-209-" and "-210-" from the bottom of
each page, respectively.
19. On page 43282. column 1. section
5.9. line 2, change "weighint" to
"weighing".
20. On page 43283, column 1, section
8.1.1. line 1. change "inital" to "initial".
21. On page 43283. column 1. section
8.2.5, line 4. change "prameters" to
"parameters".
22. On page 43283, column 2. section
8.4. line 8, remove "of the".
23. On page 43283, column 3, section
^.8.4.3. line 7, change "outsied" to
' "outside".
24. On page 43283. column 3. section
8.5. line 8, change "(S,)" to "(sp)".
25. On page 43284. column 1, section
10.1 line 7, change "Columnm" to
"Column".
26. On pages 43286. 43287, 43288. and
43289 delete the handwritten numbers "-
243-". "-244-". "-24S-", and "-246-" at the
bottom of each page, respectively.
27. On page 43291. column 1. section
5.6.3, line 2. change "issued" to "is
used".
" 28. On page 43294, column 1. section
12.7. line 14. change "volume:Volume" to
"volume:volume".
29. On page 43294. column 3, section
14.2. line 10, delete "xc".
30. On pages 43297 and 43298 delete
the handwritten numbers "-2B8-" and "-
289-" from the bottom of each of the
pages, respectively.
31. On page 43304 delete the
handwritten number "325" from the
bottom of the page.
32. On pages 43311 and 43312, delete
the handwritten numbers "-363-" and "-
364-" from the bottom of eaqh page.
respectively.
33. On page 43314. column 1. section
5.6.2. line 2. change "Supel" to "Supel-".
34. On pages 43319 and 43320. delete
typed numbers "407-" and "408-" from
the bottoms of the pages, respectively.
35. On page 43321. column 2. section
2.1. line 5. change "exchagned" to
"exchanged".
36. On page 43326. column 3. Table 3.
in the first footnote, change the
subscript ". = " to lowercase "s = ".
37, On page 43326, column 3. Table 4.
under the column heading "Single
analyst precision", line 12, change
"0.41X + 0.65" 10 '0.41 X - 0.65".
38. On page 43326. column 3. Table 4.
in the first footnote, change "X"' to
"X' ".
39. On pages 43327 through 43336.
delete the typed numbers "-451-"
through "-460-" from the bottom of each
page, respectively.
40. On page 43339, column 3, section
8.5. change "PO=90%" to "P=90%".
41. On pages 43342 and 43343. delete
the typed numbers "-496-" and "-497-"
from the bottom of each page.
respectively.
42. On page 43344. column 3. section
3.2. line 7, change "table 1" to "Table 1".
43. On page 43344. column 3. section
4.1, line 17. change superscript from
"identified*- •' to "identified4'*'.
44. On page 43349, column 3. Table 3,
line 6 under the heading "Parameter"
change syllabification from
"Benzo(b)fluo-ranthene" to
"Benzo (b)fluor-a nth ene" .
45. On page 43349, column 3, Table 4.
under column heading "Overall
precision", line 14 (Naphthalene),
change "0.41X-0.74" to "0.41X + 0.74".
46. On pages 43350 through 43352.
delete the typed numbers "-S39-"
through "-541-" from the bottom of each
of the pages, respectively.
47. On page 43357, column 2, Table l.
first three parameters, delete the space
between the prefix "Bis" and the
following parenthesis.
48, On pages 43358 and 43359. delete
the typed numbers "-S78-" and "-579-"
from the bottoms of each of the pages.
respectively.
49. On page 43361, column 1, section
6.5. line 1, change "(1.00 Mg/ML)" to
SOTOnTpige 43362Tcolumn iTsectibn"
8.2.1. line 5, change "109" to "10".
51. On page 43362. column l, section
8.2.4, lines 2 and 3, delete space between
the "/*" and the "g" to read "jtg/L".
52. On page 43364, Table 2, third
symbol explanation at the bottom of the
table, change "P.P." to "P, P,"
53. On pages 43366 and 43367. delete
the typed numbers "-614-" and "-615-"
from the bottoms of each page.
respectively.
54. On page 43368, column 2, section
3.1.1. line 2. change "cleand" to
"cleaned".
55. On page 43370, column 1. section
6.10. line 5, change "ML" to "mL".
56. On page 43370, column 1. section
7.1.1, line 9, change "n/z" to "m/z".
57. On page 43373, column 3. Table
under section 1.1. change
"Trichloroethane" to "Trichloroethene".
58. On page 43378, column 1. section
13.1. line 4, change "m/z quantitate" to
"m/z to quantitate."
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696
Federal Register / Vol. « No. 3 / Friday, Jaimary ^ Igfl5 ;
5a On page 43378, column 5. Table 4,
eighth parameter, change "1.1-
Dichloroethene'- to "1,1-
DichJoroelhane".
60. Oa page43379. Table 5. for
Toluene under the cohtma beading
Range for P. change the range from "47-
162" to "47-150".
61. On page 43373. Table 5,29th
parameter change "Tricbtoroe&ane" to
"Tricliloroetheae".
62. On page 43379, Table S, change
"Trichlorofluoromethene" to
"TrichJoroSnoram e th ane".
63. On page 43380. Table 6. change
"1.1.2=TrichloToethime" to "1,1,2-
Trichloroethane".
64. On page 43380. Table 6, for the
1.1,2-Trichteroethane, under the cohmin
heading. Accuracy, change "9.95+1.71"
to "0.950+1.71".
65. On page 43381 through 43384.
delete the handwritten •nnmbers "-704-",
"-705-", -708-", and "-707-". from the
bottom of each of the pages.
respectively.
68. On page 43386. column 2. section
6.4 line 2. change "H*SO«" to ••HsSO,",
67. On page 43386, column 3, section
7.2.2. Equation 1. put a line between the
numerator and denominator to read:
RF=
68. On page 43389. cohnnn 3. section
17; title, line 2. change "(iVATCDD)"
to "(2.3.74-TCDDJ".
69. On page 43390. column 2, Table 1.
change "Bis<2-ethylhexl) phthalate" to
"Bis(2-ethylhexyl) phthalate".
70. On page 43392. Table 7. under the
column heading "Single analyst
precision" change " Sr* " to "*,' ".
7t On page 43392. Table 7, under the
column heading "Overall precision" on
line 11. change "0.3dQx~ to "OJJOx".
72. On page 43393. Table 7. under
column heading "Single analyst
precision" change "S," " to "*r* ".
73. On pages 43394 through 43406
delete the handwritten numbers "-764-",
"-T65-". "-766-". "-"67-". ' -768-". "-
769-". "-770-", "-771-". "-77.2-". "-773-
". "-774-", "-775-", and "-7T6-" from
the bottoms of each of the pages. —
respectively.
74. On page 43409. column 1. section
7.4.2, lioe 5, insert a division sign "/"
between the two parenthesized
expressions for area to read: R=(area at
79. Oa page 43418, column 1. section
7.4.4. line 20, change "/[Rm
75. On page 43412. column t Table 1.
17th entry, change "1,1-dichlaroethajie"
to "1.1-dicHorocthene".
76. On page 43412. column 2. Table 2,
fine 8. change "Chkjroetheiw-dS"' to
-Chloroethaae-d5".
77. Oa page -43417, column Z, section
6.13, line 4. change "IJia pL" to "tflO
mL".
78. On page 43418. column 1, section
7.4.2. line 10, change "R,=Rr" to "R« >
V-
80. On page 43418. column 1. section
7.4.4. line 21, change "," to read: "R,".
41. On page 43418. column 2. section
7.5.1. line 1. add a parenthesis after C. to
read: RF=(A. X CJ/fA,, X C.J. where
82. On page 43420. column 3. section
13.4. line I, change "Massesd" to
"Masses".
83. On page 43421, column 2. section
16.2. line I. change "/Ml" to "/mL".
84. On page 43423. Table 3, 21 lines
from the bottom (EGD 372), change
detection limit from "50" to "10".
85. On page 43424. Table 3, footnote 2.
change "accepted" to "acceptable^
s=r86.-On-page-43424rtISIe'4rlifie
(EGD 184), change "ins" to "int".
87. On page 43424, Table 4. after the
footnote beginning with the word
"Column;" change "id-d." to "id.".
Appendix B to Part 136— [Corrected]
86. On page 43430, column 3. section
7.{b). secoird line after the equation,
start, the line at the left hand margin and
merge the following One to read as
follow* "calculated MDL and process
the samples through the . . .**
Appendix C to Part 138— [Corrected]
89. On page 43434. column 3. section
10.4, Hue 6. change "+5" to "±S".
•tuna caoe t$o*-oMi
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Federal Register / Vol. 50. No. 3 / Friday. January 4. 1985 / Proposed Rules
697
ENVIRONMENTAL PROTECTION
AGENCY
40 CFR Part 136
fFRL-2737-31
Guidelines Establishing Test
Procedures for the Analysis of
Pollutants Under the Clean Water Act;
Correction
AGENCY: Environmental Protection
Agency (EPA).
ACTION: Proposed rule; correction.
SUMMARY: This document corrects
proposed Guidelines Establishing Test
Procedures for the Analysis of
Pollutants that appeared at page 43437
• in the Federal Register of October 26.
1984 (49 FR 43437). FR Doc. 84-26349.
This action is necessary to correct
typographical errors.
DATES; Comments on the proposed rule
must be submitted on or before January
10,1965.
FOR FURTHER INFORMATION CONTACT:
Dr. Robert Medz, Environmental
Monitoring Systems Division, Office of
Research and Development (RD-680),
401'Nf Street. SW., Washington, D.C.
20460. Telephone Number (202) 382-
5792.
Dated: December 11.1984.
Bernard 0. Goldstein,
Assistant Administrator, Office of Research .
and Development.
The following corrections are made in
FR Doc. 84-26349 appearing on 43437 in
the issue of October 26.1984.
1. On page 43437, column 1. under
ADDRESS:, lines 3 and 4. change "Water
and Waste Management Monitoring
Research Division" to ''Environmental
Monitoring Systems Division".
2. On page 43437, column 1. under FOR
FURTHER INFORMATION CONTACT: line 3,
change "5788" to "5792".
3. On page 43437. column 2. line 1.
insert after "(GS) methods." the phrase.
"2 high pressure liquid chromotography
(HPLC) methods,11.
4. On page 43437, column 2, line 25.
change "matricies" to "matrices".
5. On page 43437, column 3. last
paragraph, line 9, change
"TetrachJoride" to "tetrachloride".
6. On page 43439, Table 1C,, parameter
10, change "Acid" to "acid"; parameter
16, change "Butyl Phthalate" to "butyl
phthalate"; parameter 42, change
"Dibromochiorobenzene" to
Dibromochloromethane".
7. On page 43440, Table 1C, parameter
85, change "Chloride" to "chloride";
parameter 86, change "Dinitrophenol" to
"dinitrophenol".
8. On page 43440. Table 1C. parameter
88. Naphthalene, under the column
heading HPLC, add "610".
9. On page 43440. Table 1C. parameter
113. delete* the hyphen between
"Tetrachloro" and "dibenzo" to read:
"2.3,7,8-Tetrachlorodibenzo-p-dioxin".
10. On page 43440, Table 1C. footnote
6. insert "Agency" after the words
"United States Environmental
Protection".
11, On page 43441, Table ID,
parameter 4, change "Atratpm" to
"Atraton" and in parameter 22. change
"Dementon-S" to "Demeton-S".
(FR Doc. 85-235 Filed 1-3-85: 8:45 am]
BfLUNO COOC 4S60-SO-M
40 CFR Part 136
[FRL-2636-6]
Guidelines Establishing Test
Procedures for the Analysis of
Pollutants
Correction
In FR Doc. 84-26349 beginning on page
43437 in the issue of Friday, October 26.
1984, make the following correction:
$136.3 [Corrected)
In § 136.3, Table ID, page 43441.
parameter 17, correct "2,4'-D" to read "2.
4-D".
tsos-oi-M
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