EPA/600/R-04/074
                                                                 July 2004
GUIDELINES FOR THE BIOREMEDIATION OF
     OIL-CONTAMINATED SALT MARSHES
                                  by

       ^ueqing Zhu, 2Albert D. Venosa, ^akram T. Suidan, and 3Kenneth Lee

                          University of Cincinnati
                           Cincinnati, OH 45221

                    2U.S. Environmental Protection Agency
                National Risk Management Research Laboratory
                           Cincinnati, OH 45268

                  3Department of Fisheries and Oceans-Canada
                      Bedford Institute of Oceanography
                      Dartmouth, Nova Scotia B2Y 4A2
                       EPA Contract No. 68-C-00-159
                             Task Order No. 8

                           Task Order Manager
                             Albert D. Venosa
                Land Remediation and Pollution Control Division
                National Risk Management Research Laboratory
                           Cincinnati, OH 45268
                National Risk Management Research Laboratory
                     Office of Research and Development
                    U.S. Environmental Protection Agency
                           Cincinnati, OH 45268

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                                     Disclaimer

The information in this document has been funded by the United States Environmental Protection
Agency (U.S. EPA) under Task Order No. 8 of Contract No. 68-C-00-159 to the University of
Cincinnati. It has been subjected to the Agency's peer and administrative reviews and has been
approved for publication as an EPA document. Mention of trade names or commercial products does
not constitute an endorsement or recommendation for use.
                                          11

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                                      Foreword

The U.S. Environmental Protection Agency (EPA) is charged by Congress with protecting the
Nation's land, air, and water resources. Under a mandate of national environmental laws, the
Agency strives to formulate and implement actions leading to a compatible balance between human
activities and the ability of natural systems to support and nurture life. To meet this mandate, EPA's
research program is providing data and technical support for solving environmental problems today
and building a science knowledge base necessary to manage our ecological resources wisely,
understand how pollutants affect our health, and prevent or reduce environmental risks in the future.

The National Risk  Management Research Laboratory (NRMRL) is the  Agency's center for
investigation of technological and management approaches for preventing and reducing risks from
pollution that threaten human health and the environment. The focus of the Laboratory's research
program is on methods and their cost-effectiveness for prevention and control of pollution to air,
land,  water, and  subsurface resources;  protection of water quality in public water  systems;
remediation of contaminated sites, sediments and ground water; prevention and control of indoor air
pollution; and restoration of ecosystems. NRMRL collaborates with both public and private sector
partners to foster technologies that reduce the cost of compliance and to anticipate emerging
problems. NRMRL's research provides solutions to environmental problems by: developing and
promoting technologies that protect  and improve the environment; advancing scientific and
engineering information to support regulatory and  policy decisions; and providing the technical
support and information  transfer to ensure implementation of environmental regulations and
strategies at the national, state, and community levels.

This publication has been produced as part of the Laboratory's strategic long-term research plan. It
is published and made available by EPA's Office of Research and Development to assist the user
community and to link researchers with their clients.
                                        Lawrence W. Reiter, Acting Director
                                        National Risk Management Research Laboratory
                                           in

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                                EXECUTIVE SUMMARY

Salt marshes are among the most sensitive ecosystems and, therefore, the most difficult to clean.
Applications of some traditional oil spill cleanup techniques in wetland habitats have caused more
damage than the oil itself. The objective of this document is to present a detailed technical guideline
for use by spill responders for the cleanup of coastal wetlands contaminated with oil and oil products
by using one  of the least intrusive approaches - bioremediation technology. This manual is a
supplement of the previously published "Guidelines for the Bioremediation of Marine Shorelines
and Freshwater Wetlands" (Zhu et a/., 2001), which has focused on the bioremediation of sandy
marine shorelines and freshwater wetlands. This guidance document includes a thorough review and
critique of the literature and theories pertinent to oil biodegradation  and nutrient dynamics and
provides examples of bioremediation options and case studies of oil bioremediation in coastal
wetland environments. It also evaluates current practices and state-of-the-art research results
pertaining to the bioremediation  of hydrocarbon  contamination, and presents a procedure for the
design and evaluation of bioremediation processes applicable to the cleanup  of oil contaminated
coastal wetlands. Special attention is given to oil bioremediation of salt marshes since they are the
most prevalent type of coastal wetland and have been the subject of the most extensive studies.

The document consists of two major parts.  Part I presents the background and  overview of
bioremediation options, which include the characteristics of coastal wetlands, oil spill threats and
countermeasures in salt marshes, and relevant state-of-the-art research. Part II provides guidelines
for design and planning of oil bioremediation in salt marshes, which includes site characterization
and evaluation, the selection of appropriate bioremediation technologies, and the design of sampling
and monitoring programs.

The overall conclusions reached by the guidance manual are as follows. Unlike sandy beaches, oil
biodegradation on marine wetlands is often limited by  oxygen, not nutrient availability. Natural
attenuation is increasingly becoming the preferred strategy  for the restoration of oil-contaminated
wetlands. However, field studies also show that on some coastal wetlands, nutrients might still be a
limiting factor for oil biodegradation, particularly  if the oil does not penetrate deeply into the anoxic
zone of the wetland sediment. When biostimulation is selected, it is recommended that nitrogen
concentrations of at least 2 to as much as 10  mg N/L should be maintained in the pore water to
achieve optimal oil  biodegradation, with  the decision on higher concentrations to be based on a
broader analysis  of cost, environmental impact, and practicality. Furthermore, if ecosystem
restoration is the primary goal rather than oil cleanup, at least one study strongly suggested that
nutrient addition would accelerate and greatly enhance restoration of the site. Abundant plant growth
took place in  the nutrient-treated plots despite the lack of oil disappearance resulting from the
addition of extra nutrients. Therefore, the decision to bioremediate a site should depend on cleanup,
restoration, and habitat protection objectives and other pertinent factors that may have an impact on
success.

No effort was made to determine the quality of secondary  data reviewed in the literature and the
conclusions made from these data.
                                            IV

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                                   TABLE OF CONTENTS

   Introduction and Overview of Bioremediation Options	1
1.1     Coastal Wetlands in the U.S	1
1.2     Oil Spills in Salt Marshes: Threats and Countermeasures	2
   1.2.1    Threats of oil spills	2
      1.2.1.1     Impact to wetland plants	2
      1.2.1.2     Impact to wildlife and ecosystems	3
   1.2.2    Response to oil spills in salt marshes	4
      1.2.2.1     Physical Methods	4
      1.2.2.2     Chemical methods	5
      1.2.2.3     In-situ burning	5
      1.2.2.4     Restoration	6
1.3     Bioremediation of Oil  Spills in Salt Marshes	6
   1.3.1    Environmental factors affecting oil biodegradation in salt marshes	6
   1.3.2    Laboratory studies	8
   1.3.3    Full-scale demonstrations	10
      1.3.3.1     Nova Scotia,  Canada, 1989	10
      1.3.3.2     San Jacinto Wetland Research Facility (SJWRF), Texas, 1994-1997	10
      1.3.3.3     Terrebonne Parish, Louisiana, 1998	11
      1.3.3.4     Gladstone, Australia, 1997-1998	11
      1.3.3.5     Nova Scotia,  Canada, 2000-2001	12
   1.3.4    Kinetics of oil biodegradation	15
   1.3.5    Monitoring biological responses to quantify the efficacy of remediation treatment	16
      1.3.5.1     Bioassessment	16
      1.3.5.2     Bioassays	17
   1.3.6    Bioremediation options on salt marshes	18
      1.3.6.1     Nutrient Amendment	18
      1.3.6.2     Microbial amendments	19
      1.3.6.3     Oxygen amendment	20
      1.3.6.4     Plant amendment (phytoremediation)	20
      1.3.6.5     Monitored natural attenuation	21
   Recommended approaches to bioremediation IN SALT MARSHES	23
2.1     Pre-treatment Assessment	25
   2.1.1    Oil penetration and oxygen availability	25
   2.1.2    Background nutrient content	26
   2.1.3    Summary of pretreatment assessment	28
2.2     Treatment Selection and Design	28
   2.2.1    Nutrient selection	29
   2.2.2    Concentrations of nutrients needed for optimal bio stimulation	30
   2.2.3    Nutrient application strategies	31
      2.2.3.1     Frequency of nutrient addition	31
      2.2.3.2     Methods of nutrient addition	31
   2.2.4    Sampling and Monitoring Plan for Bioremediation Operations	32
      2.2.4.1     Important variables and recommended measurements	32
   2.2.5    Environmental assessment of an oil-contaminated salt marsh: a case study	35
      2.2.5.1     Bioassessments	36
      2.2.5.2     Risk assessment	46
2.3     Summary and Recommendations	47
   REFERENCES	49

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1   INTRODUCTION AND OVERVIEW OF BIOREMEDIATION OPTIONS

1.1  Coastal Wetlands in the U.S.

Coastal wetlands are subjected to the influence of tidal action. They provide natural barriers to
shoreline erosion, habitats for a wide range of wildlife including endangered species, and key
sources of organic materials  and nutrients for marine communities (Boorman, 1999, Mitsch and
Gosselink, 2000). Coastal wetlands can be classified  into tidal salt marshes, tidal  fresh water
marshes, and mangrove swamps (Mitsch and Gosselink, 2000).

    •   Tidal Salt Marshes — Salt marshes are those halophytic grasslands found in the middle and
       high latitudes along protected coastlines. They are subjected to tidal action as well as high
       salinities. In the United States, they are often dominated by the grass Spartma alterniflora in
       the low intertidal zone, and Spartma patens with the rush Juncus in the upper intertidal zone.
       Most of these wetlands are distributed along the Gulf of Mexico and the Atlantic coast.

    •   Tidal Freshwater Marshes ~ These wetlands are found inland from the salt marshes but
       still close enough to the coast to experience freshwater tidal effects. Since these wetlands
       lack the salinity stress of salt marshes, they are often very productive ecosystems and
       dominated by a variety of grasses and by perennial and annual broad-leafed aquatic plants.

    •   Mangrove Swamps — Mangroves are subtropical and tropical coastal wetlands dominated
       by halophytic trees and shrubs. In subtropical and tropical regions of the world, tidal salt
       marshes give way to mangrove swamps. In the United  States, they are mostly distributed
       along the southern coast of Florida  and generally  dominated by  the red mangrove
       (Rhizophord) and the black mangrove tree (Avicennid).

It the early 1990s, it was estimated that the total area of coastal wetlands in the United States was
approximately 3.2 million ha (32,000 km2), with about 1.9 million ha or 60  percent of the total
coastal wetlands as salt marshes and 0.5 million ha as mangrove swamps (Mitsch and Gosselink,
2000).  Coastal wetlands are  no longer viewed as intertidal wastelands, and their ecological and
economic values have been increasingly recognized.  Major benefits and functions of coastal
wetlands include:

    •   Shoreline Protection - Coastal wetlands provide a buffer between land and sea, protecting
       marine shorelines from the ravages of storms and erosion by wave action. Salt marshes,
       which sustain  little damage from ocean storms, can shelter inland developed areas and
       reduce potential storm damage to coastal buildings and  structures.

    •   Support of Coastal Fisheries - Tidal marshes provide spawning site and nursery areas for
       many fish and shellfish species. Due to their high productivity, coastal wetlands produce
       great volumes of detrital organic materials and nutrients, on which many small invertebrates
       and fish feed. It is estimated that over 95 percent of the commercial fish and shellfish species
       in the United States are wetland dependent (Feierabend and Zelazny, 1987).

    •   Wildlife  Habitat - Coastal wetlands are the primary habitat for many plant and animal

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       species and provide food, water, and shelter to indigenous and migratory species. More
       importantly, wetland habitats  are  essential for the survival  of a  large percentage of
       endangered species. For example, of the 209 animal species listed as endangered by the U.S.
       Department of Interior and the U.S. Fish and Wildlife Service in 1986, about 50 percent
       depend on wetlands for their survival (Mitsch and Gosselink, 1993).

    •   Water Quality Management - Coastal wetlands maintain and improve water quality by
       acting as sediment and chemical sinks (Baker et a/., 1989). Under favorable conditions,
       wetland sediments, plants, and their associated microorganisms are able to contain, take up,
       and degrade various environmental contaminants, such as excess fertilizers, pesticides, and
       heavy metals.

Wetlands  have suffered dramatic losses as a result of human activities, such as  drainage for
agricultural use. Overall, more than 50 percent of the wetlands in the continental U. S. were lost from
the 1780s to the  1980s (Mitsch and Gosselink, 2000), and at a rate 7,300 ha/year from 1950s to
1970s (Tiner, 1984). Such losses have greatly diminished the nation's wetlands and their benefits.
The rates of loss have been declining since the mid 1970s with the enactment of wetland protection
laws and increased public appreciation.  However, threats to coastal wetlands remain,  including
conversion for agricultural,  industrial, and residential  development, mean sea level rise, and
chemical contamination from excessive nutrient inputs, chemical accumulations, and oil spills.

The threat of crude oil contamination to coastal wetlands is particularly high in certain parts of the
U.S., such as the Gulf of Mexico, where oil exploration, production, transportation, and refineries
are extensive (Lin and Mendelssohn, 1998). Oil and gas extraction activities in coastal marshes
along the Gulf of Mexico have been one of the leading causes of wetland loss in the 1970s (Mitsch
and Gosselink, 2000). Despite more stringent environmental regulations, the risk of an oil spill
affecting these ecosystems is still high because of extensive coastal oil production,  refining, and
transportation.

1.2  Oil Spills in Salt Marshes: Threats and Countermeasures

1.2.1   Threats of oil spills

Marine wetlands are especially vulnerable to oil spills because the inherently low wave energy of a
wetland does not physically remove oil effectively. They are flooded at high tide and their complex
surface can trap large amounts of oil. Impacts of oil spills to coastal wetland ecosystems have been
described and reviewed extensively (Baker etal., 1989; Fingas, 2001; NAS, 1985; Pezeshki etal.,
2000).  A brief summary on these impacts is provided in the following text.

1.2.1.1 Impact to wetland plants

Oil spills have been known to cause acute and long-term damage to salt marshes and mangroves
(Baker et a/., 1989; Burns et a/., 1993; Lin  and Mendelssohn, 1996; Pezeshki et al.,  2000). These
impacts include reduction in population  and growth rate or abnormal growth and regrowth after
initial impact. Mangroves are generally more vulnerable to oil spills than salt marshes because oil on
the partially submerged roots of mangroves interferes with respiratory activity (Duke etal., 1997;

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Evans, 1985).

The degree of oil impact also depends on various factors, such as the type and amount of oil, the
extent of oil coverage, the plant species, the season of the spill, the soil composition, and the
flushing rate. For example, No.2 fuel oil has been found to cause much higher mortality and damage
to Spartina alterniflora., a dominant salt marsh grass along the Atlantic coast and Gulf of Mexico,
than Arabian crude oil, Libyan crude oil, and No.6 fuel oil (Alexander and Webb, 1983 & 1985).
Growth of Spartina alterniflora was not significantly  affected  by oil contamination at low to
moderate concentrations (less than 5 mg crude oil/g sediment, Alexander and Webb, 1987; less than
50 mg crude oil/g sediment, DeLaune et a/., 1979) and sometimes was even stimulated (Li et a/.,
1990). However, heavy contamination by light oil can lead to widespread mortality, and plants may
require a decade or more to recover. Different wetland plants also respond differently to oil spills.
Lin and Mendelssohn  (1996) examined the effects of south Louisiana crude oil on three different
types  of coastal marshes and found that the sensitivity of these marshes to the crude oil increased in
the order of S. lancifolia  (freshwater marsh plant), S. alterniflora (salt marsh), and S. patens
(brackish marsh). Plants are more sensitive to oiling during the growing season than other periods
(Pezeshki et a/., 2000). The sediment type also plays an important role.  In general, oil  remains
longer in soils with higher organic matter and, therefore, has greater impact on resident plants. Some
wetland sediment can act  as a reservoir absorbing oil and leaching it out into adjacent coastal
habitats, causing chronic impacts on biota (Levings et a/., 1994).

1.2.1.2 Impact to wildlife and ecosystems

Oil spills on coastal wetlands not only damage plants but also have serious consequences for the
wildlife and other organisms that rely on  the wetlands as habitats and nursery grounds. These
impacts include  obvious immediate consequences, such as widespread animal mortality due to
smothering and toxic effects, and more subtle long-term effects. Oil can affect the fish population by
both direct toxicity and by a reduction in the benthic species on which they feed (NAS, 1985).
Seabirds that congregate on the salt marshes suffer from the destruction of their feeding grounds. Oil
can also change an animal's feeding and reproductive behaviors.  A light oiling  of some birds can
inhibit egg laying (Fingas, 2001). Furthermore,  heavy mortality of seabirds is often observed
because oiling effectively diminishes the natural water-repellant and insulation value of feathers.

The extent of the impacts also depends on many factors, such as the life cycle and the life habit of
organisms,  the time and season of oil spills,  the type and amount of oil,  and the duration of oil
exposure (NAS, 1985). Sediment feeders could be more vulnerable to oil than epibenthic filter
feeders. Larval fish are more vulnerable to oil than juveniles and adults. Avian mortality would be
exacerbated by a spill  occurring during their feeding and nesting  season.

Considering the different sensitivity of wetland species and populations to oil,  spills  can
significantly affect the overall balance of wetland ecosystems, especially if damage occurs to a
dominant species. On the other hand, some long-term studies have suggested that many oiled marine
wetlands could recover naturally after a long time (Baker, 1999; Hester & Mendelssohn, 2000; Sell
et a/.,  1995). Recovery times vary from a few years for some salt marshes to  over a decade for
mangroves (NAS, 1985; Sell etal., 1995). In a few extreme cases, salt marsh ecosystems have not
fully recovered decades after the initial oil spills (Baker etal.,  1993; Teal etal., 1992). The effects

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of oil on wetland ecosystems and recovery still require further investigation.

1.2.2  Response to oil spills in salt marshes

Since oil spills can cause serious damage to marine wetland ecosystems, effective countermeasures
are  essential to minimize these ecological impacts. Major oil spill response options in marine
shorelines and freshwater environments have been briefly reviewed in Chapter 1 of the  sandy
shoreline and freshwater wetland guidance document (Zhu etal., 2001). However, saltmarshes are
among the most sensitive ecosystems and, therefore, the most difficult to clean. Applications of
some traditional oil spill cleanup techniques in wetland habitats have caused more damage than the
oil itself (Baker 1999; Owens and Foget, 1982, Sell etal., 1995). Considering the characteristics of
wetland ecosystems, a number of cleanup and treatment techniques have been proposed and tested to
deal with oil contamination in coastal wetlands. The feasibility of these methods also depends on
various factors, such as the type and amount of spilled oil, season of the year, and environmental
conditions of the spill site.

1.2.2.1 Physical Methods

Many oil spill countermeasures based on physical clean up procedures, such as mechanical oil
removal, high pressure or hot water flushing, and sediment relocation, have been reported to do
more harm than good to wetland habitats. All physical methods that remain as options for use on
marine wetland environments require some caution during deployment to minimize environmental
damage.

    •  Booming and sorbents - Use of booms to contain and control the movement of floating oil
       at the edge of the wetland and removal of the oil by adsorption onto oleophilic materials
       placed in the intertidal zone. This method can be an effective strategy to prevent floating oil
       from reaching sensitive habitats with minimal physical disturbance if traffic of the cleanup
       crew is strictly controlled.

    •  Low pressure flushing - Oil is flushed with ambient-seawater at pressures less than 200 kpa
       or 50 psi to the water edge for removal (NOAA, 1992).  This technique can be used
       selectively for quick removal of localized heavy oiling with minimal damage to wetland
       vegetation. However, the potential for oil release into the sediments and adjacent water
       bodies should be considered including appropriate containment measures.

    •  Cutting vegetation— Cutting vegetation may be a useful cleanup technique to remove oils
       that form a thick coating on the vegetation and to prevent oiling of sensitive wildlife (Baker,
       1989, NOAA 1992). However, the feasibility of this method depends strongly on the season
       in which the spill occurs.  In general, winter cutting of dead  standing vegetation has little
       effect on subsequence growth, but summer cutting could cause great damage to the regrowth
       of wetland plants and result in shoreline erosion. The use of cutting should also be avoided
       immediately prior to an anticipated rise in water levels because cutting followed by flooding
       could cut off necessary oxygen to plant roots (Pezeshki et a/., 2000). Efforts should also be
       made to minimize the inevitable damage due to traffic.

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    •   Stripping - Stripping of surface sediments can cause severe environmental impacts and may
       only be considered in the case of extremely oiled wetlands where the oil in the sediments is
       likely to kill the vegetation and prevent plant regrowth. To minimize erosion and habitat
       loss, it is critical to follow the stripping by the restoration of sediment elevation and
       replanting of the wetland species (Krebs & Tanner, 1981).

1.2.2.2 Chemical methods

Chemical methods have not been widely used in the United States mainly due to the concerns over
their toxicity  and long-term environmental impacts. However, with the development of less toxic
chemical agents, the potential for their application will  increase.

    •   Dispersants - Dispersants are chemicals that promote the dispersion of floating oil from the
       water surface into  the water column. Fields  studies have shown that application of
       dispersants in near shore waters can significantly reduce the  retention of oil within the
       intertidal zone and, therefore, the impacts to wetland plants (Duke et al., 2000; Getter &
       Ballou, 1985). However, the use of dispersants  in near shore water could have short-term
       toxic  effects on adjacent coastal habitats, such as subtidal animal communities. Direct
       spraying  or contact  of dispersants with wetland plants  may also have harmful  effects on
       vegetation (Wardrop et al., 1987).

    •   Cleaners - Cleaners are chemicals that help wash oil from contaminated surfaces. These
       formulations have been used with low-pressure flushing operations to facilitate oil removal
       from wetland vegetation. Studies have shown that the application of cleaners can prevent
       mortality of salt marshes and mangroves (Pezeshki etal., 1995; Teas etal., 1993). However,
       their use has been limited because of the paucity  of data available with respect to their long-
       term effects on wetland habitats. Also, concern has been expressed over the transfer of oil to
       the nearshore waters.

1.2.2.3 In-situ burning

In-situ burning involves controlled burning of the oil and oiled vegetation at the contaminated site.
This technique is capable of rapidly removing large amounts of oil with limited equipment and
personnel. However, the technique may result in  severe damage to wetland habitats, temporary air
pollution, and possibly toxic combustion residues. The degree of impact to salt marshes is  seasonally
dependent. Like cutting, the likelihood of damage is greatest during the summer and least during the
period of dormancy in late fall and winter (Baker, 1989). In fact, fall burning of marshes has been a
commonly  used  management strategy for controlling  wetland overgrowth in many areas. The
temporary air pollution caused by the airborne emissions are generally not considered a serious
health threat or environmental concern, especially at distances greater than a few kilometers from the
fire (Fingas, 2001). Limited data and applications have indicated that in-situ burning can be a viable
option for removing a large volume of pooled oil at the  right season when sediments are saturated
(Mendelssohn etal, 1995; Pahl etal, 1997).

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1.2.2.4 Restoration

In cases of coastal wetlands being catastrophically damaged, plant and animal species have been re-
introduced as restoration strategies. (Bergen etal., 2000; Frink and Gauvry, 1995; Teas etal., 1989).
S. alterniflora was successfully replanted to restore the salt marshes in New Jersey after the 1990
Arthur Kill oil spill (Bergen et a/., 2000). Three years after the replanting, over 70% of the plant
coverage was restored as compared to only 5% by natural recolonization at the unplanted reference
sites. Mangroves were also successfully replanted to restore oil-killed mangrove forest in Panama
after the 1986 Refineria Panama oil spill (Teased a/., 1989). However, this approach may also upset
the ecological balance or natural succession processes if it is not carried out appropriately (Fingas,
2001).

1.3   Bioremediation of Oil Spills in Salt Marshes

Bioremediation is an emerging technology that involves the addition of materials (e.g. nutrients or
other growth-limiting cosubstrates)  to  contaminated  environments to accelerate  the  natural
biodegradation processes (OAT, 1991). This technology has been recognized as one of the least
intrusive methods and has been shown to be an effective tool for the treatment of oil  spills in
medium and low-energy marine shorelines (Lee et al, 1997; Swannell et al., 1996; Venosa et al.,
1996, Zhu etal., 2001). However, until a few years ago, only limited information was available on
the effectiveness and impacts of the bioremediation of oil spills in coastal wetlands (Lee etal., 1991;
Wood et a/., 1997;  Wright et a/.,  1997). Recently, several long-term field  studies on oil
bioremediation in coastal wetlands have been carried out. These studies provide better understanding
of the potential of oil remediation in such environments (Burns et a/., 2000; Garcia-Blanco and
Suidan, 2001; Jackson and Pardue, 1999; Shin et a/., 1999). In this section, an in-depth review of
current practices and research on oil bioremediation in coastal wetland environments is presented
with emphasis on the findings of these field trials.

1.3.1  Environmental factors affecting oil biodegradation in salt marshes

The  success of oil spill bioremediation depends on our ability to establish and maintain conditions
that favor enhanced oil biodegradation rates in the contaminated environment. Environmental factors
affecting oil biodegradation include temperature, nutrients, oxygen, pH, and salinity. These factors
have been discussed in general in Chapter 2 of the sandy shoreline and freshwater wetland guidance
document (Zhu etal., 2001) and in Section 5.5 of the document with respect to freshwater wetlands.
The  limiting conditions for oil biodegradation in salt marshes can be significantly different from
other marine shorelines and even freshwater wetlands. A brief summary of these conditions in salt
marshes is given here.

In terms of nutrient supply, coastal marshes are considered high-nutrient wetlands (Mitsch and
Gosselink, 2000), but most of the nutrients, and nitrogen in particular, are present in the form of
organic matter and not readily available for microbial  or plant uptake (Cartaxana et a/., 1999).
Figure 1.1 illustrates the nitrogen cycling that occurs in a wetland environment.  The amount of
inorganic nitrogen or available nitrogen for oil biodegradation will depend on many processes, such
as nitrogen fixation, nutrient mineralization, plant uptake and release, denitrification, and wetland
hydrodynamics. Studies also show that the concentration of inorganic nitrogen (mostly ammonium)

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in salt marsh sediments exhibits a seasonal pattern with a concentration peak during the summer
months probably due to higher mineralization rates associated with elevated temperatures (Cartaxana
et a/., 1999). A similar trend was also reported for available phosphorus (Nixon et a/.,  1980).
Therefore, when a major oil spill occurs in salt marshes, it is  still likely that nutrient availability
becomes a limiting factor for oil degradation, depending on the type of sediment, the season, and
quantity of oil spilled. Hence, nutrient addition may be an important remedy to contemplate when
considering any or all of these factors.
 N inflows via
 Surface water"
 groundwater
 tidal exchange
 Aerobic
 soil layer
 Anaerobic
 soil layer
                                N 9 Fixation
                                    N9 & N9O
                                                             V
N outflow via
Tidal exchange
                                      Algae & Bacteria
                                Organic N
                      NFL
          Mineralization     Nitrification

Plant Release                            NO,-  ^  Denit
                 Plant uptake
ification
             Figure 1.1 Major processes involved in nitrogen cycles in a coastal wetland
Unlike other marine shorelines, the substrates of coastal wetlands are saturated or flooded with
water, and oxygen diffusion rates through these hydric soils are very slow. As a result, available
oxygen in the soils and in the interstitial water is quickly depleted through metabolism by aerobic
organisms and chemical oxygen demand due to reduced chemical species. Typically, there is a thin
layer of oxidized soil (a few millimeters) at the surface, below which the environment becomes
anaerobic (Gambrell  and Patrick, 1978). The thickness of this oxidized layer depends on  the
population of oxygen utilizers, the rate of photosynthetic oxygen production by algae and plants, and
the rate of oxygen transport through the sediments, which is related to wind, tide and wave action. A
study of oxygen demand in an  oil contaminated  salt  marsh  sediment indicated that  oxygen
availability could be a limiting factor for oil degradation (Shin etal., 2000). These authors reported
that significant biodegradation occurred only when the tidal cycle exposed the surface of the salt
marsh to the atmosphere. The dominant electron acceptor in the anaerobic soil layer in salt marshes
is also different from most freshwater wetlands. In freshwater wetlands, methanogenesis is often the
dominant process for the oxidation  of organic carbon in the reduced soil layer, while  in marine
wetlands, sulfate reduction is usually the most important process when oxygen is limited since
seawater contains abundant sulfate (Mitsch and Gosselink, 2000). Studies have shown that in some
marine sediment, PAHs and  alkanes can be degraded under sulfate-reducing conditions at similar

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rates to those under aerobic conditions (Caldwell etal., 1998; Coates etal., 1997). The importance
of this process in the biodegradation of oil in salt marsh environments  still requires  further
demonstration, especially in the field. The inherent ability of many wetland plant species to transfer
oxygen to the rhizosphere may also play a role in reducing the effect of oxygen limitation. However,
little  research  has been  conducted  on the capacity of  this mechanism in  enhancing oil
biodegradation.

Other important environmental factors affecting biodegradation of petroleum hydrocarbons include
pH and salinity. The optimal pH for oil biodegradation is between 6 and 9 (Atlas and Bartha, 1992).
The pH of wetland sediments and the overlying water depend on both soil type and hydraulic
condition. Sediments in salt marshes and mangroves are mostly organic and often acidic. In addition,
the anoxic condition and high sulfur content in  coastal  wetlands often lead to the production of
hydrogen sulfide. When exposed to air, sulfide can be reoxidized to sulfate and result in a further
drop in sediment pH. However, in areas with frequent tidal inundation, the pH of wetland sediments
and pore water is determined by seawater and is near neutral or slightly alkaline. The salinity of pore
water in coastal wetlands may also vary  dramatically and depends on the frequency of tidal
inundation, rainfall, coverage  of vegetation, groundwater and freshwater inflow, and soil type
(Mitsch and Gosselink, 2000). In areas adjacent to coastlines or receiving frequent tidal inundation,
the salinity of wetland water is close to  that of seawater. Elevated  salinity levels are frequently
reported at higher elevations or areas with little rainfall and other freshwater supply. Brackish
marshes are frequently found in estuarine areas and other sites that extend away from the open
ocean. Salinity can significantly affect the rates of oil biodegradation. Most marine microorganisms
have an optimum salinity range of 2.5 to 3.5% and grow poorly or not at all at salinity lower than 1.5
to 2% (Zobell, 1973). Studies have also shown the rates of hydrocarbon degradation to decrease with
increased salinity above that of seawater (Rhykerd et a/., 1995; Ward and Brock, 1978).

Although many factors can affect oil biodegradation, not many environmental factors can be easily
manipulated to enhance this natural process. For example, it is not practical to alter wetland salinity,
and nothing can be done to change the climate. There are two main approaches  to oil spill
bioremediation.  (1)  bioaugmentation,  in  which oil-degrading microorganisms are added  to
supplement or augment the existing microbial population, and (2)  biostimulation, in which the
growth of indigenous oil degraders is stimulated by the addition of nutrients or other growth-limiting
co-substrates. Extensive studies  have been  carried out recently on the bioremediation  of oil
contaminated coastal wetlands both on a  laboratory scale and in the field (see next section).

1.3.2   Laboratory studies

Most of the laboratory studies have focused on the potential of using  nutrient amendments to
enhance oil biodegradation in salt marsh environments. This is because studies conducted in other
shoreline environments have demonstrated that the microbial population is rarely a limiting factor,
and nutrient addition alone had a greater effect on  oil  biodegradation than did the  addition of
microbial products (Leeetal, 1997;  Venosae^a/., 1996).

Jackson and Pardue (1999) conducted microcosm and mesocosm studies to investigate the effect of
different nutrient types on enhancing biodegradation of a Louisiana crude oil in Louisiana salt marsh
sediment. The microcosms contained a 60:1 (water/soil) slurry produced from a salt marsh sediment

-------
at an oil concentration of 0.7 g oil/g soil and were operated in a completely mixed and aerated mode,
where  oxygen  limitation  was non-existent. Nutrient species  examined  included  phosphate,
ammonium, nitrate, and phosphate plus ammonium. The results showed that oil degradation was
limited by nitrogen but not phosphorus under these conditions. Optimal nitrogen concentrations in
pore water were in the range of 100-670 mg N/L. Among the nitrogen species, ammonium was
found to be generally more effective in stimulating oil degradation than nitrate. Thus, ammonium
might be advantageous in the enhancement of the degradation of certain oil components because
ammonium is less likely to be lost from the system by washout due to its higher adsorptive capacity
to organic matter. Ammonium is also the more toxic species of nitrogen in the environment.

In a follow-on mesocosm study in the same paper (Jackson and Pardue, 1999), large intact cores
(900 cm2) of salt marsh sediments were contaminated with crude oil and treated with various
concentrations of ammonium salts. The results showed that ammonium amendments had limited
success in enhancing oil biodegradation. Even at the highest ammonium loading (10 mg/m2), the
nutrient amendment was only able to increase the degradation of lower chain length alkanes (
-------
supplemented with sodium tripolyphosphate and was added to microcosms at a N:P ratio of 5:1. The
study showed that the addition of nutrients did not enhance the rate of degradation over the natural
attenuation rate. The extent of microbial degradation of No. 2 fuel oil in all the microcosms averaged
only 20% for the total aliphatic hydrocarbons and 12% for the total PAHs. Degradation was greater
in all cases in the top layers than in the bottom layers of the columns, suggesting that oil degradation
may have been limited by oxygen availability under the conditions of this study.

Because these laboratory studies seem to suggest that adding nutrients may be effective under non-
oxygen limiting conditions, or during certain seasons,  further field experiments are necessary to
determine the potential of oil bioremediation  in coastal wetlands.

1.3.3  Full-scale demonstrations

From north temperate salt marshes to tropical mangroves, several field studies on the performance of
oil bioremediation have been carried out in recent years. These have provided more convincing
demonstrations of the effectiveness of oil bioremediation since laboratory studies may not consider
many real world conditions such as spatial heterogeneity, biological interactions, and mass transfer
limitations.

1.3.3.1 Nova Scotia, Canada, 1989

Lee  and Levy (1991) conducted one  of the first field trials on  oil bioremediation in  a salt marsh
environment. The study involved periodic addition of water-soluble fertilizer granules (ammonium
nitrate and triple super phosphate)  to enhance biodegradation  of waxy crude oil in a salt marsh
dominated by Spartina alterniflora and located in Nova Scotia, Canada (Lee and Levy, 1991). Two
levels of oil concentrations were used (0.3 and 3.0% v oil/v sediment) and two concentrations of the
NH4NO3 were tested (0.34 and  1.36 g/L sediment). In this study, pristane was used as a biomarker
for evaluation of biodegradation of crude oils. Results showed that the effectiveness of nutrient
addition was related to oil concentration.  Enhancement by fertilizer was significant at  the 0.3%
contamination level, but no enhancement occurred at 3%, which was attributed to the penetration of
the oil at higher concentrations into the reduced soil layers where little degradation is expected. This
study indicated that bioremediation might have a role  in the cleanup of coastal wetlands lightly
contaminated with oil.

1.3.3.2 San Jacinto Wetland Research Facility (SJWRF), Texas, 1994-1997

To evaluate the effectiveness of various bioremediation options, a series of field trials were carried
out in a Texas coastal wetland by a research group  from Texas A&M University (Mills et a/.,  1997;
Mills et a/.,  2003; Simon et a/., 1999; Townsend et a/., 1999; Mills et a/., 2003). This brackish
wetland was set aside for a long-term research program after an oil spill from ruptured pipelines in
1994. The 21-plot site, named San Jacinto Wetland Research Facility (SJWRF), has been used for a
series of studies on oil spill countermeasures.  Studies on oil bioremediation included three phases.
Phase I of the research evaluated the intrinsic bioremediation or natural attenuation process after the
initial oil spill. The effect of biostimulation was investigated in phase II by evaluating the use of
diammonium phosphate and diammonium phosphate plus nitrate. Phase III involved the evaluation
of two commercial bioaugmentation products and a repeated diammonium phosphate treatment. The
                                           10

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21 5 x 5 m plots were arranged in a randomized complete block experimental design, and Arabian
light and medium crude oils were used in phases II and III, respectively. Oil constituents were
determined using gas chromatography/mass spectroscopy (GC/MS) and were normalized to 17oc(H),
21(3(H)-hopane to reduce the effects of sample heterogeneity and physical losses. The results of
phase  II  showed  that the  diammonium  phosphate  treatment  significantly  enhanced  the
biodegradation rates of both total resolved saturates and total resolved PAHs, and the addition of
diammonium phosphate plus nitrate only enhanced the biodegradation of total resolved saturates
(Mills et a/., 1997). The field trial on oil bioaugmentation in phase III showed as with other
shoreline types (Leeetal, 1997a; Venosae^a/., 1996), that the addition of microbial products does
not significantly enhance oil biodegradation rates (Simon etal., 1999). However, the performance of
the nutrient treatment in this phase also failed to demonstrate the enhancement observed in Phase II.

1.3.3.3 Terrebonne Parish, Louisiana, 1998

Due to the mixed results from the earlier trials, field studies were conducted to verify the feasibility
of oil bioremediation and to determine the limiting factors in oil biodegradation in coastal wetland
environments. Shin et al. (1999 & 2000) investigated the effect of nutrient amendment on the
biodegradation of a Louisiana "sweet"  crude oil and oxygen dynamics in a Louisiana salt marsh,
which has a tidal range of 20 cm and is vegetated by Spartina alterniflora. Four treatments (unoiled
control, oiled  control, oil  plus ammonium nitrate, and  oil  plus a slow release fertilizer) were
examined in forty field plots arranged in a randomized complete block design. Oil components were
measured by GC/MS, and hopane was used as a biomarker. Oxygen dynamics were investigated by
monitoring sediment  oxygen demand (SOD), and  the  importance of sulfate reduction was
determined using a 35SO42"  radiotracer  technique. Overall, the nutrient amendments did  not
significantly stimulate oil biodegradation, which might have been related to the high background
nutrient concentrations at this site. Throughout this study, the background nitrogen concentrations in
the interstitial  pore water were higher than the threshold nitrogen concentration of 1 - 2 mg N/L
required for maximum hydrocarbon biodegradation as found by Venosa etal. (1996) in an unrelated
field trial on a sandy beach. The addition of oil and fertilizers did increase the SOD and sulfate
reduction rates in marsh soils. About 2/3 of the oxygen demand was due to aerobic respiration with
the majority of this demand exerted by hydrocarbon degrading organisms, indicating aerobic
biodegradation of the crude oil was the main mechanism. The remaining 1/3 of the oxygen demand
was attributed to sulfide oxidation. Data also showed that significant biodegradation of crude oil in
the salt marshes occurred only when the tidal cycle exposed the surface of the marsh to air (Shin et
a/., 2000). This study indicated that oxygen availability appears to control the oil biodegradation
process in salt marshes.

1.3.3.4 Gladstone, Australia, 1997-1998

A field study on the performance of oil bioremediation in both mangrove and salt marsh ecosystems
was carried out recently in a tropical marine wetland located at Gladstone, Australia (Burns et al.,
2000; Duke  et al., 2000; Ramsay et a/., 2000). This study  evaluated  the  influence of a
bioremediation protocol on the degradation rate of a medium range  crude oil (Gippsland) and a
Bunker C oil stranded in a tropical Rhizophora sp. mangrove environment and in Haloscarcia sp.
salt marshes behind the mangroves. The bioremediation strategy used in this study  involved
pumping air beneath sediment that was supplemented with a slow release fertilizer (Osmocote™
                                           11

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Tropical fertilizer) for the mangrove sites, and nutrient addition alone for the salt marsh sites. No
aeration was tested in the salt marsh experiments because the sediment of the salt marshes was much
less anoxic than that of the mangroves based on preliminary investigations. Four oiled treatments
(two types of oils with and without the bioremediation  treatments)  and two unoiled controls
(enclosure and ambient controls) were tested. Each treatment was studied with replicates of three
plots for the mangrove sites and replicates of four plots for the salt marsh sites. The oils were added
to mangrove plots and salt marsh plots at target loadings of 5 L/m2 and 2 L/m2, respectively. The
fertilizer was added at a loading of 0.15 kg/m2 40 hours after  oiling for both mangrove and salt
marsh plots and then again after three months in mangrove plots only. Aeration in mangrove plots
started 40  hr after oiling and  lasted for about four months.  In this  study,  other  than  total
hydrocarbons (THCs), only individual alkanes were analyzed using GC-FID, and phytane was used
as a biomarker. Oil analysis for the mangrove sediments over 13 months showed that no significant
change in oil composition due to biodegradation was observed until two months after oiling, and by
that time 90% of the THCs were removed from the sediments through evaporation and dissolution.
The remediation strategy did not  significantly enhance the degradation of either the  remaining
Gippsland oil or the Bunker C oil. A similar lag phase before the start of oil biodegradation was
observed in the 9-month salt marsh experiment. The addition of the fertilizer to the salt marshes did
show a stimulation of the degradation of the lighter Gippsland oil and resulted in about 20% more oil
loss as compared with the untreated plots. However, the nutrient amendment did not significantly
impact the rate of loss of Bunker C oil in the salt marsh plots. Microbial analysis for the mangrove
sediments showed that the bioremediation treatment had a significant effect on alkane degraders and
increased the population size by one to three orders of magnitude, as compared to the oil only plots.
However, the population of aromatic degraders only increased slightly (one order of magnitude).
Due to the limitation  of the experimental design, the study could  not distinguish whether nutrient
addition or aeration stimulated the microbial growth.

In the same study, Duke et al.  (2000) investigated the ecological effects of the bioremediation
strategy in  the mangroves and compared the results to a  previous field trial involving use of a
dispersant  at the  same site.  Although  the  authors suggested that the  dispersant (but not
bioremediation) significantly reduced the mortality of mangrove trees, the data appeared to show
that both treatments had some positive effects on the wetland habitats.  The increase in the tree
mortality in bioremediation plots occurred only  months after aeration and nutrient addition was
stopped. Even though some aspects of the design are questionable (e.g., lack of independent tests of
the  effect of nutrients and aeration in mangrove  environments, different  oiling  and treatment
conditions for the salt marsh and mangrove experiments), the  Gladstone field trial did provided
useful  insights on the potential of oil  bioremediation, particularly in tropical marine wetland
environments.

1.3.3.5 Nova Scotia,  Canada, 2000-2001

A comprehensive field trial conducted on oil bioremediation in a salt marsh environment was carried
out recently by the U.S. Environmental Protection Agency, University of Cincinnati, and Fisheries
and Oceans Canada in a coastal salt marsh site situated on the Eastern Shore of Nova Scotia, Canada
(manuscript not published at the time of this writing). This study explored various options for
restoring salt marshes heavily contaminated with petroleum hydrocarbons under north-temperate
conditions.  Treatment options included natural attenuation, phytoremediation, and/or bioremediation
                                           12

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by nutrient amendment and disking (gentle tilling). Like most North American salt marshes, this
tidal salt marsh was dominated by Spartina alterniflora. Tides were semi-diurnal with a range of
about 2 m. The commencement of the experiment coincided with the spring tide. Test plots for the
study were set up throughout the wetland in a way that all of them were exposed to the same tidal
inundation.

A randomized block design was used in the study. Eighteen 3 m x 3 m plots were set up in three
replicate blocks. Each block contained six treatments randomly distributed: (a) unoiled, no-nutrient
control; (b) unoiled with nutrient amendments (NfLJSTOs + CatfLiPO^iHiO}; (c) oiled with no
nutrient amendments and plants intact (naturalattenuation); d) oiled with nutrient amendments and
plants intact; (e) oiled with nutrient amendments and vegetation continually cut back to the ground
surface and removed to suppress the influence of plants and anaerobiosis associated with the
accumulation of plant detritus; (f) oiled with nutrient amendments and disked daily to introduce
oxygen into the rhizosphere.

A weathered Mesa crude oil was applied to the plots at a rate of 35 mg oil/g dry sediment during the
first two days of the study. Granular nitrogen and phosphorus nutrients were initially added to each
of the treated plots at a dosage of 450 g-N and 135 g-P per plot. Subsequent applications took place
on an as-needed basis as determined by residual nutrient analysis in the interstitial pore spaces.
When the  nitrogen levels fell below a specified concentration range of 5-10 mg N/L in the pore
water, another application of the same magnitude was made. The effectiveness of various treatments
was determined by monitoring the reduction of oil constituents in both soil and grass samples using
GC-MS techniques. Hopane was used as a biomarker to reduce the effects of sample heterogeneity
and to distinguish  bioremediation removal from physical losses. In  addition to these detailed
chemical analyses,  this project also used biological endpoints such as evidence of wetland plant
recovery   and   reduction   of   toxic  responses   to    verify   the   success   of   the
bioremediation/phytoremediation treatments (discussed in Section 2.2.4).

The study showed that the biodegradation of targeted aliphatic hydrocarbons and PAHs took place to
a very high extent at this north-temperate salt marsh. After 20 weeks, the extent of degradation of
target n-alkanes within the experimental plots averaged 87% and 97 %, respectively, for the oil in
sediment and the oil associated with emergent vegetative growth. Reduction of parent and alkyl-
substituted PAHs was about 69% in the soil samples and 88% in the plant samples. However,
targeted alkanes  and PAHs only represent a small fraction (less than 10%) of the total petroleum
hydrocarbons (TPHs). Biodegradation of TPH averaged only 3 5% in the soil samples and 42% in the
grass samples (very little of this TPH was comprised of high molecular weight plant waxes). More
than half of the applied oil remained in the marsh 20 weeks after oil application. Based on the extent
of oil washout (measured as mg hopane per kg dry soil) and the total oil loss (g TPH per kg dry soil),
the main mechanism for oil disappearance was attributed to biodegradation. These results contrast
with those reported in the St. Lawrence River freshwater wetland bioremediation study (Venosa et
a/., 2002) and the study on a tropical marine wetland at Gladstone, Australia, in which most of the
TPH was removed through physical mechanisms (Burns et al., 2000).

In this study, as  in other reported field studies, no significant differences were observed among
treatments, either  in the  degradation  of  alkanes  or PAHs.  No significant enhancement  of
biodegradation through the addition of nutrients or the use of disking was observed. The average
                                           13

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nutrient concentrations in the interstitial pore water for various treatments during this study are
summarized in Table 1.1. Data indicated that the background nitrogen (mostly ammonium nitrogen)
and phosphorus concentrations in the interstitial pore water were always far in excess of 2-5 mg N/L
and 1 mg P/L, suggesting that nutrients may not be a limiting factor for oil biodegradation in this salt
marsh. Enhanced oxygen transfer to the rhizosphere by the plants through their roots or by disking
did not appear to take place either,  at least to the level needed by hydrocarbon degraders to
metabolize the oil rapidly. From the extent of degradation of the targeted aliphatic and aromatic
hydrocarbons, it can be inferred that there was no oxygen or nutrient limitation in this particular salt
marsh site.

Table 1.1 Average nutrient concentrations in pore water for different treatments during
Nova Scotia study

NH4-N
mgN/L
NO3-N
mgN/L
PO4-P
mgP/L
Treatment A
Background
9.43
0.09
1.25
Treatment
B
Nutrient
Control
60.63
28.57
12.42
Treatment
C
Natural
Attenuation
18.08
0.07
2.17
Treatment D
Phyto-
remediation
92.49
37.11
5.66
Treatment E
Nutrient
Amendment
80.83
30.56
9.42
Treatment F
Disking
104.6
28.89
14.75
However, nutrient addition did stimulate microbial growth, as in the Gladstone study (Ramsay etal.,
2000). Alkane degraders in this wetland seemed to be nutrient limited, since the addition of nutrients
without oil led to an increase in number of about two orders of magnitude relative to background
levels. However, when oil was  added to the plots without any  nutrient amendment  (natural
attenuation plots), the increase in alkane degraders was also on the same order, suggesting the
existence of different populations that can degrade alkanes under different conditions. However,
PAH degraders were clearly limited by their carbon sources. Only oiled plots showed an increase in
the number of PAH degraders. These populations did not seem to be limited by nutrients since the
addition of nitrogen and phosphorus did not have an effect on either the number of microorganisms
or on the rate of PAH degradation.

In summary, these field trials suggest that nutrient amendments may be less effective in stimulating
oil biodegradation rates in coastal wetlands than sandy beaches. Oil biodegradation on marine
wetlands is often limited more by oxygen than by nutrient availability. A large fraction of the total
nutrients in wetland sediments is bound in organic matter (i.e., plants and detritus) that is not readily
available for microbial uptake. In such cases, natural ongoing mineralization processes may provide
an effective means to overcome this restraint. However, field experience also suggests that some
coastal wetlands may be nutrient limited, and in these cases, biostimulation with nutrient enrichment
may still be an appropriate countermeasure treatment if the oil does not penetrate deeply into the
anaerobic layer of the wetland sediments (Lee and Levy,  1991; Venosa et a/.,  2002; Mills et a/,
1997).
                                           14

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1.3.4   Kinetics of oil biodegradation
Knowledge of the kinetics of oil biodegradation is important for assessing the potential fate of
targeted compounds,  evaluating the efficacy  of bioremediation, and determining  appropriate
strategies to enhance oil biodegradation. The rates of biodegradation vary greatly among the various
components of crude oils and petroleum products and depend on many environmental factors, such
as temperature, nutrient concentration, and oxygen content. The heterogeneity of oil distribution on
shorelines or wetland sediments makes kinetics studies even more difficult. To reduce the variability
associated with heterogeneous oil distribution, Venosa etal. (1996) utilized hopane normalization in
studying the kinetics of oil biodegradation and developed first-order biodegradation rate constants
for resolvable alkanes and important two- and three-ring PAH groups present in a light crude oil on a
sandy beach in the Delaware field study. The first order relationship was expressed as:
                                                                                 (1.1)
where (A/H) is the time-varying hopane-normalized concentration of an analyte, (A/H)0 is that
quantity at time zero, and k is the first-order biodegradation rate constant for analyte, A.

Tablel.2 Summary of first order biodegradation rate constants from field studies
Field
Study
Location
Delaware
Quebec
Canada

Texas




Louisiana
Nova
Scotia
Canada
Shoreline
Type
Sandy
beach
Tidal
freshwater
wetland
Brackish
wetland



Salt marsh
Salt marsh

Oil Type
Bonny light
crude oil
Mesa light crude
oil

Phase II:
Arabian light
crude oil
Phase III:
Arabian medium
Crude oil
South Louisiana
crude oil
Mesa light crude
oil

Treatment
Control
Nutrient
Inoculum
Control
Nutrient

Control
Nutrient
Control
Nutrient
Inoculum
Control
Nutrient
Control
Nutrient

First order biodegradation rate
day'1
Alkanes
0.026
0.056
0.045
0.0028
0.0023-0.0034

0.019
0.042-0.061
0.020
0.024
0.019-0.030
0.005
0.005
0.020
0.026-0.039

PAHs
0.021
0.031
0.026
0.0028
0.0016-
0.0041
0.017
0.018-0.027
0.015
0.013
0.016-0.017
N/A
0.010
0.011-0.013

Reference
Venosa et
al., 1996
Venosa et
al, 2002

Simon et al.,
1999



Shin et al.,
1999
Unpublished
data

Since the Delaware study, several field trials conducted in other types of environments, including
salt marshes and a freshwater wetland, have reported first-order oil biodegradation rate constants
obtained using the same approach (Shin et al., 1999; Simon et al., 1999; Venosa et al., 2002). The
results of these kinetic studies in the field are summarized in Table 1.2. It can be seen that except for
                                            15

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Phase II of the San Jacinto field study (Mills etal., 1997; Simon etal., 1999), nutrient amendments
did not show significant biodegradation rate enhancements in most of these wetland environments.
Nonetheless, it is encouraging to see that crude oils can be biodegraded intrinsically on marine
wetlands at similar rates as on sandy beaches (i.e., the Delaware site). The higher intrinsic oil
biodegradation rates  reported for salt marshes when compared to freshwater wetlands may be
attributed to the generally greater oxygen limitation in freshwater wetland environments (Mitsch and
Gosselink, 2000). It should be noted here that in the St. Lawrence River freshwater wetland study
(Venosa et al., 2002), the oil was manually raked into the sediment, causing penetration of oil into
the anaerobic zone. It is not known whether higher biodegradation rates would have ensued had this
raking not been done.

1.3.5   Monitoring biological responses to quantify the efficacy of remediation treatment

In addition to the demonstration that remedial treatments reduce the concentration of residual oil, it
is necessary to demonstrate that they do not produce any undesired environmental and ecological
effects. As discussed in the sandy shoreline and freshwater wetland guidance document (Zhu etal.,
2001), two complimentary approaches are available: (1) bioassessments, which typically monitor
changes in populations and communities of flora and fauna (Herri cks and Schaeffer, 1984); and (2)
bioassays, which include toxicity tests and bioaccumulation studies (Chapman, 1989).

1.3.5.1 Bioassessment

The monitoring of alterations in benthic community structure is frequently used to assess the
potential impacts of residual oil within sediments. For example, in a follow up of the Exxon Valdez
oil spill clean up, Driskell etal. (1996) noted negative effects including reductions in size, biomass,
fecundity, and increased  mortality as a result of hot water washing. Changes in epifauna and infauna
were also used to assess the rates of natural recovery and the impacts of intertidal clean-up activities
on the coast of Saudi Arabia following the  1991 Persian Gulf oil spill (Watt et al., 1993). The
possibility of adverse ecological effects such as algal blooms and invertebrate  mortality from
excessive nutrient amendments associated with bioremediation treatments is also a concern (Lee,
2000a; Lee et al, 2001a, 2001b).

To date,  sediment bioassessments have been  largely based on the tracking  of changes in
macroinvertebrate community  structure. For a holistic  approach,  it is recommended that
consideration should also be given to the bioassessment offish and other non-benthic community
organisms (e.g.  bacteria, phytoplankton, cladocera, and amphibians). Furthermore, with recent
advances in biotechnology, micro-scale bioassays are now available to monitor alterations at the
subcellular or multicellular level of biological organization (Lee etal., 1998; Wells etal., 1998). In
wetland environments, quantification of potential impacts on vegetative growth  can be used to
document the efficacy of bioremediation strategies. For example, in a tidal freshwater wetland
experiment, the predominant plant species (Scirpuspungens) was reported to be tolerant to the oil,
and its growth was significantly enhanced above that of the  unoiled control by  the addition of
nutrients (Lee et al., 200la). Monitoring of recolonization  within impacted areas  should be
considered as an endpoint in bioassessments, as it provides integrated information on the impact of
contaminants on processes such as immigration, emigration, competition, and predation.
                                           16

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1.3.5.2 Bioassays

As discussed in the sandy shoreline and freshwater wetland guidance document (Zhu et a/., 2001),
acute and/or chronic bioassays can be performed on whole sediment (e.g., solid-phase), suspended
sediment, sediment liquid phases (pore water, interstitial water), or sediment extracts (elutriates,
solvent extracts).  Since various forms of biota differ in their sensitivity to toxicants, it is highly
recommended that a test battery approach with species from different trophic levels be utilized in
environmental assessments to ensure ecological relevance.

Sediment bioassays have been used extensively to diagnose the effect of oil spills (Teal etal., 1992;
Gilfillanefor/., 1995; Neff and Stubblefield, 1995; Randolph etal., 1998) and their counter-measures
such as bioremediation (Lee et al., 1995b; Mearns et al.,  1995; Mueller et al., 1999). Criteria to
consider for the selection of bioassays include: (1) sensitivity to test material, (2) ecological and/or
economic relevance, and (3) the availability of regional expertise for the analysis and interpretation
of results.

1.3.5.2.1   Numerous bioassays can be  used to  document the impact of oil  spills in coastal
environments. Benthic invertebrates such as amphipods and shellfish have been found to be highly
sensitive to residual hydrocarbons  following oil spill incidents (Teal et al. 1992; Gilfillan et al.,
1995; Mueller at al., 1999; Wolfe et al.,  1996). They have been used in both field and laboratory
studies to monitor the impact and effectiveness of oil spill countermeasures such as bioremediation
(Mearns et al., 1997, 1995; Lee et al., 2001a,b). In terms of quantifying a microbial response, the
Microtox test is based on the measurement of changes in light emission by a nonpathogenic,
bioluminescent marine bacterium (Vibriofisherf) upon exposure to test samples.  This commercial
assay has been used by regulatory agencies for toxicity screening of chemicals, effluents, water and
sediment, and for contamination surveys and environmental risk assessment, and its application for
monitoring the efficacy of oil spill remediation methods has been proven (Lee et al., 1995b, 1997;
Mueller etal, 1999).

1.3.5.2.2   Due to their economic,  recreational, and aesthetic value,  fish have been  historically
selected as a primary bioassay organism. Biochemical  and physiological alterations induced by
toxicant exposures can result in:  1) anatomical changes, 2) structural alterations in organelles, cells,
tissue,  and organs, and 3)  alteration of metabolic processes. For example,  the observation of
neoplasms in fish was one of the first histopathological indices used in ecotoxicology. Biomarkers,
defined as biochemical, physiological, or pathological responses measured in individual organisms
on exposure to environmental contaminants, such as mixed function oxidase (MFO) reactions (Ortiz
de Montellano,  1986) are also used. MFO reactions induced by PAHs and a variety of halogenated
hydrocarbons are highly sensitive to contaminants. In the tidal freshwater wetland study with early
life stages offish, Hodson et al. (2001) noted that oil alone, oil mixed with sediments in the lab, and
oiled sediments from the experimental plots all caused induction of MFO (CYP1 A) enzyme activity
relative to unoiled controls, indicating the presence and bioavailability of PAH. Induction did not
vary markedly among treatments, but declined slowly with time. Concomitant chemical analysis
suggested that PAHs were depleted primarily by weathering or sediment dispersion rather than by
bioremediation treatments.

To date, detrimental effects from nutrient enrichment have not been observed following full-scale
                                           17

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field operations (Prince, 1993; Mearns etal., 1997). However, field experiments have suggested that
the possibility of detrimental effects from bioremediation treatments cannot be fully discounted
(Mueller etal., 1999). For example, oxygen depletion and production of ammonia from excessive
applications of a fish-bone meal fertilizer during one field experiment caused detrimental effects that
included toxicity and the suppression of oil degradation rates (Lee et a/., 1995a). Furthermore, in a
subsequent bioremediation field trial it was reported that a commercial bioremediation product
suppressed the rates  of toxicity reduction as it increased the retention of residual oil within the
sediments (Lee et a/., 1997). Bioassays used to document the effectiveness of bioremediation
treatments in sandy intertidal shoreline sediments oiled with a weathered light crude oil showed an
inhibitory effect on the hatching of grass shrimp due to the addition of nutrients (Mearns et a/.,
1995). Furthermore, most recently, in the tidal freshwater study described in the sandy shoreline and
freshwater wetland guidance document (Zhu et al. , 200 1), it was noted that amphipod toxicity levels
became elevated during the study due to excessive nutrient enrichment (Lee et a/., 2001a). It is
recommended that future operational guidelines include ecotoxicological-monitoring protocols.

1.3.6  Bioremediation options on salt marshes

Major bioremediation options have been described in the sandy shoreline and freshwater wetland
guidance document (Zhu et al., 2001).  This document provides a summary of the most current
information on restorative techniques pertaining to salt marshes.

1.3.6.1 Nutrient Amendment

As stated in previous  sections, biostimulation has been ineffective in accelerating the disappearance
of oil on certain oil-contaminated salt marshes (Garcia-Blanco and Suidan, 2001; Shin etal., 1999)
due  to either  the presence of high background nutrient concentrations or oxygen limitation.
However, a few field studies did show enhanced oil biodegradation through nutrient addition (Lee
and Levy, 1991; Mills et a/.,  1997); therefore, nutrient amendment may still be a viable  option for
removing hydrocarbons  from an oil-contaminated wetland when nutrients are limiting. Nutrients
used for biostimulation can be classified as water-soluble, slow-release, oleophilic, and organic.

    •  Water-soluble nutrients — Commonly used water-soluble nutrient products include mineral
       nutrient salts (e.g. KNO3, NaNO3, NH3NO3, K2HPO4, MgNH4PO4), and many commercial
       inorganic fertilizers (e.g. the 23 :2 N:P garden fertilizer used in Exxon Valdez case). They are
       usually applied in the field through the spraying of nutrient solutions or spreading of dry
       granules. Compared to  other types of nutrients, water-soluble  nutrients are more readily
       available and  easier to manipulate to maintain target nutrient concentrations in interstitial
       pore water. The main disadvantage is that they are more likely to be washed away by tidal
       and wave action. However, this washout effect is of lesser concern in salt marshes,  since
       they generally represent low-energy environments that are subj ect to little turbulent mixing.
       A field study on nutrient hydrodynamics showed that water-soluble nutrients could remain in
       contact with oiled sediments for weeks on low energy shorelines before being washed out
               ^a/., 1997a; Harris et al., 1999).
    •   Slow-release fertilizers — Slow release fertilizers are normally available in solid forms that
       consist of inorganic nutrients coated with hydrophobic materials like paraffin or vegetable
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       oils or organic nutrients encapsulated by semi-permeable or controlled-rate degradable
       surface coatings. They are designed to overcome the washout problems and provide a
       continuous supply of nutrients to oil contaminated areas. This approach may also cost less
       than adding water-soluble nutrients due to less frequent applications (Lee et al., 1993). The
       Gladstone field trial has shown promise for the application of slow-release fertilizers in
       coastal wetlands (Burns etal, 2000). In this study, the degradation of a Gippsland crude oil
       in salt marsh plots was stimulated by the addition of Osmocote™, a slow release fertilizer
       consisting of a mixture of inorganic nutrients coated with an organic resin.

    •   Oleophilic nutrients - Another approach to overcome the problem of water-soluble nutrient
       washout is to utilize oleophilic organic nutrients. The  rationale for this strategy is that oil
       biodegradation mainly occurs at the oil-water interface, and since oleophilic fertilizers are
       able to adhere to oil and provide nutrients at the oil-water interface, enhanced biodegradation
       should result without the need  to increase nutrient concentrations in the bulk pore water.
       Results have been mixed. Some studies have suggested that oleophilic fertilizers might be
       more suitable for use in high-energy, coarse-grained environments due to poor penetration of
       fine sediments by oleophilic fertilizers (Sveum et al.,  1994;  Sveum and Ladousse, 1989).
       Bioremediation agents containing organic substrates such as meat and fish-bone meal and
       yeast extracts may have the capacity to provide essential micro-nutrients and organic growth
       substrates that may be limiting. However, the large amount of organic carbon within this
       type of amendment may also cause problems. For example, the organic carbon in the product
       may be biodegraded by microorganisms preferentially over petroleum hydrocarbons, thus
       contributing to oxygen depletion and resulting in undesirable anoxic  conditions (Lee and
       Levy, 1987,1989; Lee  etal, 1995a,b; Swannelle^a/., 1996). Considering their high cost and
       lack of demonstrated  effectiveness, oleophilic fertilizers are unlikely to be the choice
       biostimulation agent for oil cleanup in coastal wetlands.

1.3.6.2 Microbial amendments

Addition of oil-degrading microorganisms (bioaugmentation) has been proposed as another type of
bioremediation strategy. The  rationale for this approach includes the contention that indigenous
microbial populations may not be capable of degrading the wide range of substrates that are present
in complex mixtures such as petroleum  and  that seeding may reduce the lag period before
bioremediation begins (Leahy and Colwell, 1990). Although many vendors of microbial agents
claim that  their  product aids the  oil biodegradation process based on laboratory tests, the
effectiveness of microbial amendments has not been convincingly demonstrated in the field (Zhu et
al., 2001). Actually, results from most field studies indicate that bioaugmentation is not effective in
enhancing oil biodegradation on marine shores. Field  studies conducted on  sandy beaches have
shown that  nutrient addition or biostimulation alone had a greater effect on oil biodegradation than
microbial seeding (Lee and Levy, 1987; Lee et al., 1997, Venosa et al., 1996). The San Jacinto
study, the only reported field  trial on oil bioaugmentation  in a coastal wetland environment, also
revealed that addition of microbial products did not significantly enhance oil biodegradation rates
(Simon et al., 1999). This is because hydrocarbon-degrading microorganisms  are ubiquitous in the
environment, and their density can increase by many orders of magnitude after exposure to crude oil,
as evidenced in recent studies  of coastal wetlands (Garcia-Blanco and Suidan,  2001; Ramsay etal.,
2000; Townsend etal., 1999).  Also, added bacteria may not be able to compete with the indigenous,
                                           19

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well-adapted population (Lee and Levy, 1989; Venosa etal., 1992). The mass of the hydrocarbon-
degrading bacterial population on coastal wetlands is also limited by factors that are not affected by
an exogenous source of microorganisms, such as predation by protozoans, the oil surface area, or
scouring of attached  biomass by  tidal activity. Therefore,  it is  unlikely that exogenous
microorganisms would persist in contaminated wetlands even when they are added in large numbers.
As a result, microbial amendments will not have any long-term or  short term      beneficial effects
in shoreline cleanup operations.

1.3.6.3 Oxygen amendment

Because wetland soils are inundated with water, the diffusion rates of oxygen through the soils are
very slow, and oxygen in the interstitial water is quickly depleted by aerobic metabolism of detritus
that is abundant in wetlands. A few centimeters, and often only a few millimeters below the
sediment surface, the wetland sediments are anaerobic. Therefore, oxygen is likely a limiting factor
for oil biodegradation in marine wetlands. However, an appropriate technology for increasing the
oxygen concentration in such environments, other than reliance on the wetland plants themselves to
pump oxygen down to the rhizosphere through the root system, has yet to be developed. Many of the
oxygen amendment technologies developed in terrestrial environments (e.g. tilling, forced aeration,
and the addition of chemical oxidants), are currently not considered viable options for use in coastal
wetlands. There is concern that their deployment is expensive  and environmentally  intrusive.
Furthermore, their effectiveness in  enhancing oil biodegradation in wetland environments is
unproven.

The Gladstone field trial showed that a forced aeration strategy was only able to increase the depth
of the aerobic layer of the wetland sediments from 1 mm to 2 mm, and could not significantly
stimulate oil biodegradation in the anaerobic mangrove environment (Burns etal., 2000). Strategies
involving the mixing of  surface sediments, such as tilling or disking, have also been proven
ineffective  in recent field studies (Garcia-Blanco and Suidan, 2001; Garcia-Blanco et a/., 2001b;
Venosa et a/., 2002). Not only does this approach cause severe ecological damage to wetlands, it
also enhances  oil  penetration deep  into  the  anaerobic  sediments,  resulting  in slower oil
biodegradation. As for adding alternative electron acceptors, there is  no strong evidence yet to
suggest that the addition of nitrate as an electron acceptor can enhance oil biodegradation when
oxygen is  limiting (Garcia-Blanco  and Suidan,  2001; Townsend et a/., 1999). The  high oil
degradation rates under sulfate-reducing conditions found in some laboratories (Caldwell et a/.,
1998; Coates etal., 1997) have not been convincingly demonstrated in the field. Therefore, further
research is still  required to  explore  cost-effective oxygen amendment techniques for the
bioremediation of coastal  wetlands.

1.3.6.4 Plant amendment (phytoremediation)

Phytoremediation,  the stimulation of contaminant degradation by the growth of plants and their
associated  microorganisms, is emerging as a  potentially cost-effective  option  for cleanup of
petroleum hydrocarbons  in terrestrial environments (Banks et a/., 2000; Frick et  a/., 1999a).
Mechanisms responsible for oil phytoremediation may include degradation, containment, and the
transfer of contaminants from soil to the atmosphere (Cunningham etal., 1996). Frick etal. (1999b)
indicated that the primary loss mechanism for petroleum hydrocarbons is the degradation of these
                                           20

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compounds by microorganisms in the rhizosphere of plants. Phytoremediation was hypothesized to
be particularly effective when used together with nutrient enrichment because hydrocarbon
contamination may result in nutrient deficiencies in contaminated  soil. Added fertilizers could
increase  the  rate  of oil degradation by indigenous  microorganisms in the rhizosphere and
simultaneously stimulate  plant biomass production,  thereby  increasing the effectiveness  of
phytoremediation and accelerating the recovery of the affected wetland plant ecosystem.

Extensive studies have been conducted  on the phytoremediation of petroleum hydrocarbons in
terrestrial environments (Frick etal. 1999a,b). Researchers at University of Saskatchewan, Canada,
recently  developed a catalogue of plants with the  potential  to phytoremediate hydrocarbon
contaminated soils following a review of information in the literature and the conduct of field
surveys (Godwin etal., 1999; and Frick etal.,  1999c). Nevertheless, only limited studies have been
carried out on the effectiveness of phytoremediation in enhancing oil degradation in coastal wetland
environments. Lin and  Mendelssohn (1998) found in a greenhouse study that  application  of
fertilizers in conjunction with the presence of salt marsh and brackish marsh transplants significantly
enhanced oil degradation. In another mesocosm study, Dowty etal. (2001) evaluated the effects of
soil organic matter content, plant species, soil oxygen status and nutrient content on oil degradation
and plant growth  response in fresh marsh environments. The study  found that the amount of oil
remaining after 18 months was lowest in aerated and fertilized mesocosms containing either/1.
hemitomon or S. lancifolia and a substrate of low organic matter content. Field studies, however,
have not demonstrated such significant effects as in the mesocosm studies. A recent Nova Scotia
field  trial showed that  addition of nutrients  did not result in  significant enhancement  of
biodegradation of crude  oil, whether or not plants were left intact or removed (Garcia-Blanco and
Suidan, 2001). Similar results were also found in the St. Lawrence River freshwater wetland field
study (Garcia-Blanco etal., 200 Ib; Venosa etal., 2002). On the other hand, the results of these field
trials did suggest that although application of fertilizers in conjunction with the presence of wetland
plants may not significantly enhance oil degradation, it could accelerate habitat recovery. There is
evidence that nutrient amendments could stimulate vigorous vegetative growth, reduce sediment
toxicity and oil bioavailability (Lee etal, 2001a).

In summary, on the basis of field trials conducted to date, the effectiveness of phytoremediation in
enhancing oil degradation in coastal wetlands is highly site-specific and does not promise to be an
effective oil cleanup technique per se. However, it does show promise in accelerating the recovery
and restoration of wetland environments contaminated with oil  and oil  products, which is  the
ultimate goal of the treatment.

1.3.6.5 Monitored natural attenuation

Natural attenuation has been defined as the reliance on natural processes  to achieve site-specific
remedial objectives (USEPA, 1999). When used as a clean up method, a monitoring program is still
required to assess the performance of natural attenuation. This approach is increasingly viewed as
the most cost-effective, although the least cosmetically appealing, option for the cleanup of oil spills
in coastal wetland environments since it causes the least adverse ecological impacts often associated
with cleanup activities (Baker, 1999; Owens etal, 1999; Sell etal, 1995). Sell etal. (1995); Mills
et al, 2003) compared the rates of recovery between treated and untreated wetlands based on 20
case studies of heavily oiled salt marshes.  They concluded that most traditional cleanup methods did
                                           21

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not promote significant long-term ecosystem recovery.

Recent field studies on oil bioremediation have demonstrated that the availability of oxygen, not
nutrients,  is often the limiting factor for oil biodegradation in coastal wetlands. However, as
discussed earlier, no  feasible technique is currently available for increasing the  availability of
oxygen in such an environment. Fortunately, these field studies also showed that  the natural
biodegradation of alkanes and PAHs could occur to a very high extent and at similar rates in coastal
wetlands as in sandy beaches (See section 1.3.4). Therefore, in consideration of the potential impacts
associated with physical clean-up procedures in wetlands (i.e. trampling), natural attenuation should
be given more preference in decision making for oil  spill cleanup in coastal wetlands when the oil
concentration is not high enough to destroy the ecosystem.
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2   RECOMMENDED APPROACHES TO BIOREMEDIATION IN SALT MARSHES

Existing studies have demonstrated that oil biodegradation on marine wetlands is often limited by
oxygen, not nutrient availability. Natural attenuation is increasingly becoming a promising and even
a preferred strategy for the restoration of oil-contaminated wetlands. However, field studies also
showed that on  some  coastal wetlands,  nutrients might  still be  a limiting  factor for oil
biodegradation, particularly if the oil does not penetrate deeply into the anoxic zone of the wetland
sediment (Lee and Levy, 1991; Mills etal., 1997; Venosa etal., 2002).  Therefore, biostimulation
with nutrient  amendment can still be  an appropriate countermeasure treatment under some
circumstances. General guidelines for the bioremediation of oil-contaminated marine shorelines,
which are mostly derived from studies and practices on sandy beaches, have been presented in the
sandy shoreline and freshwater wetland guidance document (Zhu et a/., 2001). Although the general
principles for achieving successful oil bioremediation for all types of marine shorelines are the same,
a simple transfer of response strategies may not be necessarily the most appropriate since salt marsh
habitats are significantly different from other marine situations. Therefore, guidelines and special
considerations for oil bioremediation in coastal wetland environments are presented here based on
current understandings and field studies, particularly the findings of the Nova Scotia field study
(Garcia-Blanco and Suidan, 2001).

Similar to the general protocol presented in the sandy shoreline and freshwater wetland guidance
document (Zhu et al., 2001), a general procedure or plan for the selection and application of
bioremediation technology in  salt marshes is illustrated in Figure 2.1.  The major steps in  a
bioremediation selection and response plan include:

   1.  Pre-treatment assessment - This step involves the evaluation of whether bioremediation is
      a viable option based on the biodegradability of the spilled oil, the depth of oil penetration
      and oxygen availability, concentrations of background nutrients,  the presence of
      hydrocarbon-degrading microorganisms, the type of shoreline substrate, and other logistic
      and environmental factors (pH, temperature, remoteness of the site, accessibility of the
      site and logistics,  etc.).

   2.  Design of treatment and monitoring  plan - After the decision is made to use
      bioremediation, further assessments  and planning are needed prior to the application. This
      step  involves selection of the rate-limiting treatment agents (e.g., nutrients), determination
      of application strategies for the rate-limiting agents, and design of sampling and
      monitoring plans.

   3.  Assessment and termination  of treatment - After the treatment is implemented according
      to the plan, assessment of treatment  efficacy and determination of appropriate treatment
      endpoints are performed based on chemical, lexicological, and ecological analysis.
This document will focus on the operational guidelines for decision-making and planning of oil
bioremediation in  salt marshes. Guidelines with respect to the assessment of field results  and
establishment  of appropriate treatment endpoints can be found in the Chapter 6 of the  sandy
shoreline and freshwater wetland guidance document (Zhu et al., 2001).
                                           23

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                                        Step 1:
                                Pretreatment Assessment
      Oil
      biodegradability
Oil penetration
and oxygen
availability

^
\
>
Background
nutrient content

>
Climate, prior oil
exposure and other
site characteristics

T

                                     Ifbioremediation
                                     is selected
                                        Step 2:
                                Bioremediation Planning
        Nutrient products
Nutrient application
strategy
Sampling and
monitoring plan
                                        Step 3:
                             Assessment and Termination
       Analysis of oil biodegradation
       and physical loss
                  Toxicological and ecological
                  analysis
Figure 2.1 Procedures for the selection and application of oil spill biore mediation in salt marshes
                                             24

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2.1  Pre-treatment Assessment

Major considerations in the assessment of the need for biostimulation in salt marshes include the
evaluation  of 1)  oil types and  concentrations, 2) oil  penetration and  oxygen availability 3)
background nutrient content, and 4) other environmental factors such as the prevalent climate and
prior oil exposures. Among these factors, the assessments of oil penetration, oxygen availability and
background nutrient content are of particular importance for bioremediation of salt marshes and will
be discussed in following sections.  Detailed discussion on the assessments of oil types  and
concentrations, oil biodegradability, climate and other environmental factors can be found in the
sandy shoreline and freshwater wetland guidance document (Zhu et a/., 2001).

2.1.1   Oil penetration and oxygen availability

Unlike other types of marine shorelines (e.g. sandy beaches), the most important limitation for
cleanup of an oil-contaminated marine wetland is oxygen availability. Wetland sediments become
anoxic often below a few millimeters to centimeters of the soil surface. When substantial penetration
of spilled oil into anoxic sediments has taken place, available evidence suggests that biostimulation
with nutrient addition has limited potential for enhancing oil biodegradation, and it would likely be
best simply to leave it alone and not risk further damage to the environment by trampling and the
associated  bioremediation activities. Therefore, the  evaluation of oil penetration  and oxygen
availability is probably the  most important  pre-treatment assessment for determining whether
bioremediation is a viable option.

The thickness of the oxidized layer within wetland sediments varies from  a few millimeters to
several centimeters, depending on the population of oxygen utilizers, the rate of photosynthetic
oxygen production by algae, the soil chemical composition, and the rate of oxygen transport into the
wetland sediments (Mitsch and Gosselink, 2000; Shin etal, 2000). For example, soil organic matter
is a major oxygen sink in salt marshes and, therefore, oxygen deficiency is more likely to occur in
wetland soil with high organic matter content. Oxygen  limitation will be less severe in the area
where the wetland surface is exposed to the atmosphere or is subjected to strong surface mixing by
convection currents and wave action.

The depth of the aerobic layer can be identified through both visual observation and measurements
of DO and redox potential. The wetland surface or the  aerobic layer is often a brown or brownish-
red color due to the presence of ferric ions. The anoxic zone in wetland sediments is  either bluish
gray due to the presence of ferrous ions or, more often in salt marshes, black along with a foul odor
associated with the production of hydrogen sulfide under sulfate reducing conditions. Anoxic
conditions  can also be determined by measuring dissolved oxygen in pore water. Oxygen will
become a limiting factor when DO concentration in pore water approaches zero. When using DO
probe, a reading of 0.1 or 0.2 mg/L indicates the depletion of dissolved oxygen. Redox potential is a
more  sensitive measurement of the  degree  of  reduction of wetland  sediments. For example,
denitrification occurs  at a  redox  potential of approximately 250 mV and sulfates are reduced to
sulfides at a redox potential between -100 and -200 mV (Mitsch and Gosselink, 2000).

The depth of oil penetration also depends on many factors, such as oil type, concentration and
shoreline substrate. In general, fresh crude oils and heavy oils tend to adhere to the marsh surface
                                           25

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sediment or pool on the sediment surface. Light oils and oil components can generally penetrate the
top few centimeters of wetland sediment. However, penetration can be much deeper into burrows
and cracks extending up to one meter (NOAA, 1992). A microcosm study on the penetration of
weathered light Arabian crude oil in freshwater wetland sediments showed that the oil was able to
penetrate about 2.5 cm in 16 weeks for both a flooded condition and a saturated but non-flooded
condition (Purandare, 1999). However, the amount of the oil able to penetrate into the sediment was
much less for flooded sediments, where most of the oil floated on the surface of the water. The depth
of oil penetration also increases with the increase of oil  concentration and therefore affects the
potential of oil biodegradation. In the field trial reported by Lee and Levy (1991), the rates of oil
degradation  in  the salt marsh were not stimulated by nutrient amendments at the  higher test
concentration (3.0%  v oil/v sediment), where oil penetrated to  anaerobic layers of sediment.
However, bioremediation was effective at the lower test concentration (0.3 % v oil/v sediment),
where the oil did not penetrate beyond the aerobic sediment surface layers. In the same field study,
Lee and Levy (1991) also examined the effect of oil concentration on a sandy beach and found that
oil biodegradation rates were enhanced by the nutrient amendment at the higher oil concentrations
(3%), where oxygen was not a limiting factor. The result suggested that the favorable concentrations
for using bioremediation would be much lower in salt mashes than on sandy beaches.

The type of shoreline substrate is another important factor affecting the oil penetration and the
feasibility of using bioremediation.  Shoreline substrate can affect oil  penetration from  the
perspectives of both  the sediment texture and the soil  chemical  composition.  Generally, oil
penetrates coarse sediments more readily than fine sediments.  However, because the texture of all
wetland sediments is normally very fine, the substrate chemical composition plays a more important
role in oil penetration in  salt marsh environments.  Studies  have  shown  that the rates of oil
penetration and biodegradation are strongly related to the soil organic matter content (Dowty etal.,
2001; Lin and Mendelssohn, 1996).  Oil is more likely to penetrate into sediments with higher
organic content since it associates more readily with organic matter than with mineral particles. In a
greenhouse study, Lin and Mendelssohn (1996) investigated the performance of oil biodegradation
in three types of coastal wetlands - salt, brackish, and freshwater marsh. They found that the rates of
oil degradation were highest in the salt marshes and lowest in the freshwater marshes. The difference
in oil residue was mainly attributed to the difference in the soil organic content, which was lowest in
the salt marsh sediments and highest in the freshwater marsh sediments. The study also measured the
concentrations of the  oil that penetrated the soils in digested  (to  remove the associated organic
matter) and undigested marsh soil and found that the oil concentrations were 41 -279 times higher in
the undigested soil than the digested one. Similar results were observed by Dowty etal. (2001) in a
mesocosm study  conducted in fresh marsh  environments.  They  found  that the  rates of oil
degradation  were significantly higher in  the inorganic sediments than the organic ones under
different oil  concentrations and nutrient levels. These results are  consistent with the notion that
oxygen demand is higher and oil is more readily able to penetrate into organic sediments. Therefore,
oil bioremediation seems more likely to be successful when applied in a wetland with lower organic
matter content.

2.1.2   Background nutrient content

To  determine whether nutrient  amendment is a viable  option, it  is necessary to assess  the
background nutrient levels in the contaminated site, particularly the nutrient concentrations within
                                           26

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the interstitial water in that environment.  There is no need to add nutrients if natural nutrient
concentrations are high enough to sustain rapid intrinsic rates of oil biodegradation. However,
because oxygen is often the determining factor in oil  degradation on  coastal  wetlands,  the
assessment of background nutrient concentration is important and needed only after the assessments
of oil  penetration and oxygen availability  conclude that oxygen limitation is  not  a serious
impediment. In other words, when substantial oil penetration into the anoxic zone of the wetland
sediments occurs, nutrient amendment is not likely to be effective even if nutrient deficiency exists.
As shown in the St. Lawrence River field trial (Venosa etal., 2002), the average pore water nitrogen
concentration in natural attenuation plots was only about 0.74 mg N/L, well below the levels needed
for maximum hydrocarbon biodegradation (Venosa etal., 1996). However, the dramatic increase in
nutrient levels in the biostimulation plots did not enhance oil biodegradation above that achievable
in the natural attenuation plots due to the oxygen limitation within that freshwater wetland sediment.

However, when oxygen availability is not a limiting factor, the decision to use nutrient amendments
should be based on how high the natural levels are relative to the optimal or threshold nutrient
concentrations. It has been recommended in the sandy shoreline and freshwater wetland guidance
document (Zhu et al., 2001) that the threshold concentration for optimal hydrocarbon biodegradation
on marine shorelines is in the range of 2 to 10 mg N/L based  on the field experiences on sandy
beaches (Bragg et al.,  1994; Venosa et al.,  1996) as well as in an estuarine environment (Oudet et
al., 1998). Although no  such threshold concentration has been experimentally identified in  salt
marsh environments, recent field experiences did provide some insights. The Nova Scotia study
found that the average background nitrogen concentration in pore water was about 10 mg N/L at the
experimental  site. Thus, nitrogen limitation was not an important factor (Garcia-Blanco and Suidan,
2001). The ineffectiveness of nutrient amendments in enhancing oil biodegradation under this high
background nutrient level suggested that the nitrogen threshold concentration should be lower than
10  mg  N/L.  However,  the San Jacinto  River study suggested that  the threshold  nitrogen
concentration may be higher than 2 mg N/L on coastal wetlands. During Phase II of the study,
nutrient addition apparently enhanced  oil degradation  even when  the background  nitrogen
concentration was about 5 mgN/L (Harris etal, 1999; Mills etal., 1997). This study, however, was
inconclusive because the  same enhancement  was not observed when the treatment was repeated
during the following year (Simon etal., 1999). Although further research is still needed, it appears
from existing evidence that the threshold nitrogen concentration for optimal oil biodegradation in
salt marshes is likely similar to that obtained in other shoreline types (e.g. 2-10 mg N /L).

The investigation of background  nutrients should also determine whether the present nutrient
concentrations are typical of the area or sporadic (i.e., determine the impact of chronic runoff from
nearby agricultural practices and local industrial and domestic effluents). As described in Part I,
coastal marshes are generally considered high-nutrient wetlands. However, inorganic bioavailable
nutrient concentrations in salt marsh  sediments may  exhibit a strong seasonal pattern with a
concentration peak usually during the summer months probably due to a high mineralization rate at a
higher temperature (Cartaxanae^ al., 1999; Nixon et al., 1980). The available nutrient levels can also
be elevated as a result of runoff, fire and death of plants. If these  events are sporadic, biostimulation
may still be appropriate when the nutrient levels fall below threshold concentrations.
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2.1.3   Summary of pretreatment assessment

Based on the current understandings discussed in the previous sections as well as in the sandy
shoreline and freshwater wetland guidance document (Zhu et al., 2001), the following pretreatment
assessments should be conducted to determine whether bioremediation is a viable option in response
to a spill incident in salt marsh environments:

   •   Determine whether the spilled oil is potentially biodegradable - Light petroleum products
       and light crude oils (API gravity > 30°) are relatively biodegradable; products rich in normal
       alkanes are also relatively biodegradable; heavy crude oils (API gravity < 20°) and residual
       fuel oils, which are high in polar compounds (asphaltenes and resins) are less biodegradable.
       High concentrations of oil (of any weight) may also inhibit biodegradation. For details, see
       Zhu etal. (2001).

   •   Determine whether oxygen is a factor limiting oil biodegradation by measuring the depth of
       oxidized sediment layer and the extent of oil penetration - When a substantial portion of the
       spilled oil has penetrated into anoxic sediments, biostimulation with nutrient addition has
       limited potential for enhancing oil biodegradation. Oxygen limitation is less likely to occur
       in wetland sediments with lower organic matter and/or contaminated with oil at moderate
       concentrations.

   •   Determine whether the nutrient content at the impacted area is likely to be a limiting factor
       by measuring the background nutrient concentrations within the interstitial water in that
       environment - If oxygen is not the limiting factor, the decision to use bioremediation by
       addition of nutrients should be based on how high the natural levels are relative to the
       optimal or threshold nutrient concentrations (e.g., > 5 mg N/L).  It should also be determined
       if the natural nutrient concentrations present are typical of the area or sporadic. If sporadic,
       biostimulation may still be  appropriate when the nutrient levels fall to limiting values; if
       chronic, biostimulation may not be necessary.

   •   Determine whether climatic or seasonal conditions are favorable for using bioremediation -
       Bioremediation may  be more  effective during  warmer  seasons, particularly  in  cold
       environments, since oil biodegradation rates are higher during these seasons. However, this
       does not necessarily mean that summer is the most favorable season. Because inorganic
       nutrient levels in salt marsh sediments often peak during the summer, biostimulation will not
       be effective if the nutrient content is no longer the limiting factor during warmer seasons.
       Prior exposure to oil will also be a favorable but not a solely determinative condition for
       selecting bioremediation.

2.2   Treatment Selection and Design

If biostimulation by nutrient addition is determined to be a potentially effective cleanup option based
on the pretreatment assessments, further evaluation and planning are needed before its application.
This  step involves  selection of the rate-limiting  nutrients, determination  of optimal nutrient
concentrations and application strategies, and design of sampling and  monitoring plans.
                                            28

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2.2.1   Nutrient selection

One of the  first tasks during the  stage of treatment selection and design would be to select
appropriate nutrient products. The laboratory treatability tests, especially well-designed microcosm
or mesocosms tests,  are most commonly used approaches to  determine the type and level of
amendments. However, responders will likely not have time or resources to  conduct a treatability
study. This section, therefore, serves to support a reasonable approach to deciding which type of
formulation to use.

Screening and treatability tests that have been reported in the literature involve the determination of
rate limiting nutrients as well as optimal forms of nutrient species. Nitrogen, phosphorus, or both can
limit oil degradation in salt marshes. In a microcosm study, Jackson and Pardue (1999) found that
nitrogen but not phosphorus was the rate-limiting nutrient for oil degradation in sediment from a
Louisiana salt marsh. Wright et al. (1996, 1997) reported the opposite result for a mesocosm study
where oil degradation was mainly limited by the concentration of phosphorus in sediment from a
Texas salt marsh.

The molecular form  of nutrients is  also important. For example, although  both ammonium and
nitrate are  capable  of  enhancing  oil  degradation when nitrogen  is  a limiting factor,  their
effectiveness may  differ depending on  the type of oil and the properties of shoreline substrate.
Jackson and Pardue (1999) found that addition of ammonium appeared to stimulate degradation of
crude oil more effectively than nitrate in salt marsh soils in a microcosm study. The ammonium
requirement was only 20% of the concentration of nitrate to  achieve the  same increase in
degradation. The authors concluded that ammonium was less likely to be lost from the microcosms
by washout due to its higher adsorptive capacity to sediment organic matter. A recently completed
study at a salt marsh in Nova Scotia also showed that the ammonium spikes after nutrient addition
were always substantially higher than the nitrate spikes, even though the only exogenous source of
nitrogen was NH4NO3 (Table 1.1). The lower pore water nitrate concentrations can be attributed to
the higher washout rate for nitrate and its loss through denitrification within the  anoxic sediments.
Under such  circumstances, ammonium based nutrients may be superior to nitrate based nutrients
because the  nutrient dosage will be much lower when using ammonium than nitrate to achieve the
same pore nitrogen concentration. However, this may not always be the case. Actually, the St.
Lawrence River field study showed that the pore water nitrate concentrations were always higher
than the ammonium concentrations after NELtNOs was added (Venosa etal., 2002). This finding was
attributed to the adsorption of NH4+ onto the negatively charged soil particles and its uptake by the
root systems of the wetland plants. This result also suggests that the effects of nitrate washout and
denitrification were less important in this fresh water marsh.

Nutrient selection might also be influenced by temperature conditions. In a field study, Lee et al.
(1993) investigated the efficacy of water-soluble inorganic fertilizers (ammonium nitrate and triple
super phosphate) and  a slow release fertilizer (sulfur-coated urea) to enhance the biodegradation of a
waxy crude oil in a low energy shoreline  environment.  The results showed  that at temperate
conditions above 15°C, the slow-release fertilizer appeared to be more effective in retaining elevated
nutrient concentrations within the sediments and more effective in enhancing oil degradation than
water-soluble fertilizers. However, lower temperatures were found to reduce the permeability of the
coating  on the slow-release fertilizer and suppress nutrient release rates. Water-soluble fertilizers
                                           29

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such as ammonium nitrate were then recommended under these temperature conditions. Based on
the above discussion, it is recommended that, if temperature conditions allow use of slow-release
fertilizer (i.e., temperatures in excess of 15°C), then that would be the preferred fertilizer to use in a
salt marsh. If the temperature were lower, then ammonium nitrate would be appropriate. In either
case, the amount of fertilizer to use should be based on maintenance of a minimal amount that would
not limit biodegradation (i.e., something greater than about 5 mg N/L and 0.5 mg P/L).

In addition to demonstrating the efficacy of nutrient products in enhancing oil degradation, it is also
critical to demonstrate that bioremediation products have low toxicity and do not produce any
undesired environmental and  ecological  effects,  especially when  applied to such  sensitive
ecosystems as salt marshes. Various toxicity test protocols have been discussed in part I as well as in
the sandy shoreline and freshwater wetland  guidance document (Zhu etal, 2001). A case study on
the assessment of bioremediation treatment through monitoring biological responses in an oil-
contaminated salt marsh will also be presented later in this document.

2.2.2   Concentrations of nutrients needed for optimal biostimulation

Since oil biodegradation largely takes place  at the interface between oil and water, the effectiveness
of biostimulation depends on  the nutrient concentration in the interstitial  pore  water of oily
sediments (Bragg etal., 1994; Venosa etal.,  1996). The nutrient concentration should be maintained
at a high enough level to support maximum oil biodegradation based  on the kinetics of nutrient
consumption. Higher  concentrations will provide no added benefit but may lead to potentially
detrimental ecological and toxicological impacts.

Only  a few studies have been reported on the optimal nutrient concentration  in salt marsh
environments.  In a microcosm study using salt marsh sediment slurry, Jackson and Pardue (1999)
found that oil degradation rates could be increased with increasing concentrations of ammonia in the
range of 10 - 670 mg N/L, with most of the consistent rate increases occurring between 100 -670 mg
N/L. They further proposed a critical nitrogen concentration range of 10-20 mg N/L. Harris et al.
(1999) examined the nutrient dynamics during natural recovery of an  oil-contaminated brackish
marsh and found that there was an interdependency between the natural nutrient levels and the extent
of oil degradation when the background nitrogen concentration in pore water declined from 40 mg
N/L to 5 mg N/L. Evidence from bioremediation field studies also suggested that concentrations of
approximately 5 to 10  mg/L of available nitrogen in  the interstitial pore water is sufficient to meet
the minimum nutrient requirement of the oil  degrading microorganisms (Garcia-Blanco and Suidan,
2001; Mills et al.,  1997; See Section 2.1.2). As mentioned earlier, the threshold concentration range
for optimal hydrocarbon biodegradation on marine shorelines is around 2 to 10 mg N/L  based on
field experiences on sandy beaches (Bragg et a/., 1994;  Venosa et  a/., 1996) and in an estuarine
environment (Oudet et al., 1998). The apparent higher threshold nitrogen concentrations in salt
marshes are mainly due to the lack of information with respect to oil biodegradation under lower
nitrogen concentrations, since all the existing field  studies were conducted in salt marshes with
background nitrogen concentrations of at least 5 mg N/L (Garcia-Blanco  and Suidan, 2001; Harris et
al., 1999; Mills etal., 1997; Shin etal., 1999). Therefore, it is reasonable to recommend, as for other
types of shorelines, that biostimulation of oil impacted salt marshes should occur when nitrogen
concentrations of at least 2 to as much as to  5-10 mg N/L are maintained in the pore water with the
decision on higher concentrations to be based on a broader analysis of cost, environmental impact,
                                           30

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and practicality. In practice, a safety factor should be used to achieve target concentrations, which
will depend on anticipated nutrient washout rates, selected nutrient types, and application methods.
The safety factor used in salt marsh environments may generally be smaller than that used in higher
energy beaches due to the reduced degree of nutrient washout expected in salt marshes. One needs
always to keep in mind, however, that nutrient toxicity might exist if too much nutrient is applied to
a coastal wetland (Mueller et al., 1999). The factors that lead to higher nutrient losses in wetland
environments may also be important, such as sediment adsorption, plant uptake, and denitrification
(if applicable).

2.2.3   Nutrient application strategies

Once the optimal nutrient concentrations have been determined, the next task is to design nutrient
application strategies, which include nutrient application frequency and delivery methods.

2.2.3.1 Frequency of nutrient addition

The frequency of nutrient addition to maintain the optimal nutrient concentration in the interstitial
pore water mainly depends on shoreline nutrient loss rates.  A tracer study conducted on a low-
energy beach and a high-energy beach in Maine demonstrated the influence of shoreline types on
nutrient washout rates (Wrenn et a/., 1997a; Zhu et a/., 2001)). The study shows that during spring
tide, nutrients can be completely removed from a high-energy beach within a single tidal cycle. But
it may take more than two weeks to achieve the same degree of washout from a low-energy beach.
Washout during the neap tide can be much slower because the bioremediation zone will be only
partially covered by water during this period. Salt marshes are low-energy systems and nutrient
washout rates in such environments should be similar to the observations made on the low energy
beach in the Maine study. In salt marshes, the washout rates may be further reduced when using
ammonium-based nutrients due to their higher affinity to adsorb onto the sediment as compared to
nitrate-based fertilizers (Jackson and Pardue, 1999). Therefore, weekly to monthly additions may be
sufficient for biostimulation of salt marshes when the nutrients are applied during neap tide. It is
even possible that only one nutrient dose is required for the bioremediation of some coastal marshes.
A study on the nutrient dynamics in an oil contaminated brackish marsh showed that it took more
than one year for nutrient concentrations to decrease to background levels after being naturally
elevated by flooding and perturbations due to the spill (Harris etal., 1999). However, this may not
be truly indicative of nutrient application dynamics, since exogenous nutrients were not added in this
case. Nutrient sampling, particularly in sediment pore water, must be coordinated with nutrient
application to ensure that the nutrients become distributed throughout the contaminated area and that
target concentrations are being achieved. The frequency of nutrient addition  should be adjusted
based on the nutrient monitoring results.

2.2.3.2 Methods of nutrient addition

Nutrient application methods should be determined based on the characteristics of the contaminated
environment, physical nature of the selected nutrients, and the cost of the application. In many
intertidal environments, particular high-energy shorelines, the primary consideration in developing
and selecting a nutrient application method has been how to overcome the washout problems. Many
attempts have been made in this regard, including the use of slow release and oleophilic fertilizers

-------
(Prince, 1993) and the subsurface application of nutrients (Wise et a/.,  1994). However, since
nutrient washout in  coastal wetland  environments is relatively slow, the  more  important
considerations in such cases should be on the use of less expensive and less  environmentally
intrusive application methods. As discussed in the sandy shoreline and freshwater wetland guidance
document (Zhu et a/.,  2001), current experience indicates that surface application of dry granular
fertilizer (either slow-release or water-soluble) to the impact zone at low tide is probably the most
cost-effective and less environmentally intrusive way to control nutrient concentrations.

2.2.4   Sampling and Monitoring Plan for Bioremediation Operations

2.2.4.1 Important variables and recommended measurements

Important variables to be monitored in an oil bioremediation project include the environmental
factors that limit oil  biodegradation rates (e.g., temperature, interstitial nutrient and oxygen
concentrations),  evidence of oil biodegradation (e.g.,  concentrations of oil and its components),
microbial activity (e.g., bacterial numbers and activity), and toxicological effects. Primary variables
recommended for monitoring of bioremediation field programs in coastal wetland environments are
listed in Table 2.1.

If pretreatment assessments determine that oil biodegradation in the field is likely to be limited by
nutrient rather than oxygen availability, pore water nutrient analysis becomes  one of the most
important measurements in developing proper nutrient addition strategies and assessing the effect of
oil  bioremediation. The  frequency of nutrient sampling must  be coordinated with nutrient
application. This is to make certain that (1) the treatment is reaching and penetrating the impact
zone, (2) target concentrations of nutrients are being achieved, and (3) toxic nutrient levels are not
being reached. The location from which nutrient samples are collected is also important. Recent
research on solute transport in the intertidal zone has shown that nutrients may remain in the beach
subsurface for much longer periods than in the bioremediation zone (Wrenn etal.,  1997b). Nutrient
concentration profiles along the depth of the oil-contaminated region may be monitored by using
multi-port  sample wells  or by  the  extraction  of sediment  samples collected from the oil-
contaminated region (Venosa  et a/., 2002; Lee et a/., 2001a). The sampling depth should be
established from the results of site surveys to determine the maximum depth of oil penetration. To
counter the inherent heterogeneity observed in field studies,  a positive "margin of error" should be
added to ensure that the samples will encompass the entire oiled depth throughout the project. The
sampling depth must be modified if observations during the bioremediation application suggest that
the depth of oil penetration  has changed.

The success of oil bioremediation will be judged by  its ability to reduce the concentration and
environmental impact of oil in the field.  As discussed in Chapter 3 of the sandy shoreline and
freshwater wetland guidance document (Zhu et a/., 2001), to effectively monitor biodegradation
under highly heterogeneous conditions, it is necessary that concentrations of specific analytes (i.e.,
target alkanes and PAHs) within the oil be measured occasionally using chromatographic techniques
(e.g., GC/MS) and are reported relative to a conservative biomarker such as hopane. However, from
an operational perspective, more rapid and less costly analytical  procedures are also needed to
satisfy regulators and  responders on a more real time, continual basis. Existing protocols for the
measurement of TPH, especially those using infrared absorption of Freon-extracts, are generally not
                                           32

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reliable and have limited biological significance. Using GC/FID and integrating the area under the
chromatogram is better. TLC-FID appears to be a promising screening tool for monitoring oil
biodegradation (Stephens et a/., 1999), although not enough experience is available to make any firm
recommendations on its use at this time.

As suggested in the foregoing paragraph, GC/MS operated in the selected ion monitoring mode
(SIM) is the preferred method to use to assess the progress of biodegradation. One sampling per
month of composited samples from the site analyzed by GC/MS should suffice to provide evidence
that hydrocarbons are being biodegraded. To this end, normalization of biodegradable constituents in
the oil to hopanes, steranes, and/or other potential biomarkers (e.g., highly substituted 4- or 5-ring
PAHs like C4-chrysene) is essential to ensure  that the disappearance  observed is due to the
bioremediation  action rather than  physical  washout.  Samples  are  normally  extracted with
dichloromethane and cleaned up using column chromatography prior to conducting the GC/MS.
However, due to the expense and expertise involved with GC/MS analysis, more frequent analysis of
TPH is appropriate to follow the temporal progress of treatment. It is suggested that at least one TPH
sampling event per week be conducted at the spill site. Either the gravimetric or GC/FID method of
TPH analysis should be used. Interpretation of chromatographic methods may be confounded by the
presence of plant lipids and other biogenic compounds present in the environment; thus, care should
be exercised in interpreting results. For example, plant lipids normally give rise to peaks in the
chromatograms at retention times that coincide with odd-numbered higher molecular weight alkanes
in the range of €25, C2?, C29, Csi, and €33. Thus, it is essential that the chromatogram of the spilled
oil be known to compare to actual  samples analyzed.

In addition to monitoring treatment efficacy, the bioremediation  monitoring  plan should also
incorporate reliable ecotoxicological endpoints to document treatment effectiveness for toxicity
reduction.  Commonly used ecotoxicity monitoring techniques, such as the Microtox® assay and an
invertebrate survival bioassay, have also been summarized in the sandy shoreline and freshwater
wetland guidance document (Zhu et a/., 2001). These micro-scale bioassays may provide an
operational endpoint indicator for bioremediation activities on the basis of toxicity reduction (Lee et
a/.,  1995b). A summary of criteria for selecting an appropriate bioremediation endpoint based on
both oil degradation and toxicity reduction has been presented in the sandy shoreline and freshwater
wetland guidance document (Zhu etal., 2001). Examples for a salt-marsh study are presented in the
following  sections.
                                           33

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Table 2.1 Monitoring plan for an oil bioremediation project in a coastal wetland environment
Analysis
*Dissolved nitrogen
Dissolved phosphorus
*Residual oil
constituents
* Total petroleum
hydrocarbons
Redox and sulfide
*Dissolved oxygen of
pore water
pH of pore water
Microbial populations
Microbial activity
*Toxicity of residual
oil
Shoreline profile
Matrix
Sediment
(interstitial
pore water)
Sediment
(interstitial
pore water)
Sediment
Sediments
Sediment
(interstitial
pore water)
Aqueous
Aqueous
Sediment
Sediment
Sediment,
pore water
Contaminated
site
Recommended Methods
Extract in acidified 0.1% NaCl.
4500-NH3 H (Automated
Phenate Method) and
4500-NO3" F (automated Cd-
reduction)
Extract in acidified 0.1% NaCl.
4500-P E (ascorbic acid method)
Extract into dichloromethane
(DCM).
Analyze components by GC/MS-
SIM
Gravimetric analysis
(dichloromethane extraction) or
GC/FID analysis of DCM
extracts.
Redox and sulfide electrodes
Hach high range assay
Potentiometric with combination
electrode
MPN for alkane and PAH
degraders
Genetic biomarkers
Uptake/respiration of
radiolabelled substrates.
In-situ respiration
Biotests (e.g. Microtox Test,
Amphipod survival test, MFO
induction, etc.)
Intertidal/supratidal zone surveys
using fixed benchmarks at the
study site. (e.g., wells, plot
boundary markers).
References
Eaton etal., 1995
Page etal, 1986
Eaton etal, 1995
Page etal, 1986
Venosaetal, 1996
NET AC, 1993
ATI Orion,! 99 la,b
Hach Company,
Loveland, CO
Page etal, 1986
Wrenn and Venosa,
1996
Macnaughton et al.,
1999
Lee and Levy, 1989
Prince et al, 1999
See Section 1.3.5
and 2.2.4.2
Wrenn et al, 1997a,b
* Critical measurements
The sandy shoreline and freshwater wetland guidance document (Zhu et al., 2001) presents other
important variables in a comprehensive monitoring plan, including site background conditions (e.g.,
oxygen, redox, pH, sediment grain size, and temperature) and shoreline profiles. Oxygen availability
                                           34

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is crucial for rapid bioremediation since hydrocarbon biodegradation is primarily an aerobic process.
Although the pretreatment assessments may have determined that oxygen availability might not be a
serious concern for the on-going project,  oxygen limitation is always a potential problem in a
wetland environment. Therefore, dissolved oxygen (DO) in the pore water should be monitored on a
regular basis. The frequency of DO sampling should also be coordinated with nutrient application,
particularly when organic nutrients are used (Lee et a/.,  1995b; Sveum and Ramstad, 1995; See
Section 4.1.3), to insure that anoxic conditions do not result. When available oxygen does become
limiting, the nutrient dosage and application frequency should be adjusted accordingly. Monitoring
oil penetration and analyzing redox potential and sulfide concentrations with depth of wetland
sediments will assist in determining whether oil  has penetrated into the anoxic zone during the
process of bioremediation. This assessment can also be used as a criterion in determining treatment
endpoints.

Measurement  of pH  in the pore water is also important in monitoring oil bioremediation.
Biodegradation of oil in marine environments is optimal at a pH of about 8 (Atlas and Bartha, 1992).
The pH of seawater is usually around 8.5, which is adequate to support rapid oil biodegradation. For
accurate interpretation of field data, analysis of sediment grain size should be conducted to verify
study site homogeneity.

2.2.5  Environmental assessment of an oil-contaminated salt marsh: a case study

Since environmental assessment is a relatively new approach in evaluating the effectiveness of oil
bioremediation treatments,  a case study outline is presented as a means to provide  operational
guidance to spill responders. This example is based on  a controlled oil spill field trial recently
conducted in a salt  marsh at Conrod's Beach, Nova Scotia, Canada, to determine if bioremediation
by nutrient enrichment or phytoremediation by enhanced plant growth would accelerate the rates of
residual oil loss and habitat recovery. The experimental design and bioremediation performance with
respect to oil biodegradation has been reviewed (Section 1.3.3).  Standard bioassessment and biotest
procedures (Section 1.3.5)  were used to quantify the rates of habitat recovery  and to identify
detrimental treatment effects (e.g., toxicity of the bioremediation agent or oil degradation by-
products). The overall success of the remedial operations was  based on the integration of results
from a suite of assays, which were chosen on the basis of ecological relevance to the site of concern,
cost  considerations, and the availability of technical expertise (Venosa and Lee, 2002).
                                           35

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2.2.5.1 Bioassessments.

2.2.5.1.1  Recovery of vegetation. Growth (biomass) of the predominant plant species (Spartina
alterniflord) within the salt marsh was significantly suppressed by oiling, and recovery was not
observed during the first growing season. While initial results showed some recovery in all oiled
plots in the following spring, there was also evidence of changes in species composition within the
treated plots. Another opportunistic plant species that was more tolerant to the altered site conditions
increased its percentage of cover. By the end of the second growing season, the treated plots showed
substantial evidence of recovery in the sections of the plots that were not removed by sampling.

2.2.5.1.2  Microbial responses.

    •   Oil degradation potential. Potential hydrocarbon degradation rates of representative alkane
       and PAH components within sediment  samples  were determined  by quantifying the
       respiration  rate of  added 14C-labelled  hexadecane  and 14C-labelled phenanthrene  as
       representatives of w-alkane and PAH class components within the test oil (Lee and Levy,
       1989, Caparello and LaRock 1975, Walker and Colwell, 1976). Time-series changes (Week:
       4, 7,  9, 12,  16, 20) in the turnover time of these specific tracers were calculated with the
       actual concentrations of residual hexadecane and phenanthrene in each sample determined
       by GC/MS to account for dilution by the unlabelled fraction of the specific substrates under
       study.

       Results of the added 14C-labeled hexadecane studies clearly illustrated the stimulation of
       indigenous  organisms with the potential to degrade alkanes within the first 10-weeks after
       the application of oil (Figure 2.2). The lower the turnover time, the greater is the stimulatory
       effect (lower turnover times mean higher biodegradation rates). A stimulatory  effect  on
       potential hexadecane degradation rates by the addition of nutrients to unoiled sediments was
       also observed. However, within the oiled sediments, remedial treatments based on nutrient
       additions did not appear to cause a stimulatory effect that could be adequately resolved by
       measurement of hexadecane respiration rates. Natural attenuation (Treatment C: oil without
       nutrients in the figure) appeared to be relatively effective. These radiotracer studies are in
       agreement with detailed chemical analysis that showed that 87% of the target w-alkanes were
       degraded in the test sediments within 20 weeks. Similar observations were made for the
       biodegradation of PAHs (represented by phenanthrene,  a  3-ringed poly cyclic  aromatic
       hydrocarbon) with the exception that nutrient amendments to the unoiled control sediments
       had no stimulatory effect (Figure 2.3) as contrasted with the hexadecane results. These
       observations are in full agreement with the corresponding field studies on microbial growth
       by MPN analysis. It was noted that besides oil, the addition of nutrients to unoiled plots also
       resulted in  an increase in the number of potential w-alkane degraders by two orders of
       magnitude with respect to background levels. Only oiled plots showed an increase in the
       number of PAH degraders.

    •   Denitrification activity. Denitrification is a primary  process that regulates the nitrogen cycle
       in wetland sediments (Figure 1.1). Microbial  denitrification activity was monitored on each
       sampling occasion by placing a gas chamber on each plot and taking headspace samples over
       a 30-minute period, which were subsequently analyzed for nitrous oxide, an intermediate in
                                           36

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       the denitrification of nitrate. The seasonal average denitrification activity, plotted against
       treatment type showed that in all cases where nutrients were applied (Treatments D = oil +
       nutrients, E = oil + nutrients + cut plants, F = oil + nutrients + disking), there was a net
       positive denitrification potential (Fig. 2.4). Natural attenuation (Treatment C: oil without
       nutrients) and Treatment A (unoiled control) showed a net negative denitrification potential.
       These results indicate that nutrient application resulted in increased denitrification activity in
       the sediments.
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                                             37

-------
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                                           38

-------
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Figure 2.4. Seasonal average in denitrification activity with different treatments from Conrod's
Beach sediments from June to November, 2000. Letter designations are the same as in Figure 2.2.

•  Structural deformity ofForaminifera. For ecological relevance in the monitoring of potential effects
   in contaminated environments, it is preferred to use native (indigenous) species as indicators. In this
   study, Foraminifera (forams), single-celled microorganisms (protozoa) that construct a shell from
   available mineral particles or secrete one of calcium carbonate or of silica, were found to be a unique
   indicator species, due to their sensitivity to residual oil. This is attributed to the fact that the process
   of forming their shell has been reported to be highly susceptible to certain types of environmental
   pollution resulting in deformities. Foram skeletons are also resistant to decay, and many are found as
   fossils. Having these properties, foram tests and deformities can be used to monitor the ecological
   effects of oil spills and treatments.
                                            39

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    The forams under observation at the study site were typically between 63-500 |im. They occurred in
    the sediment at an abundance of 400-4000 species per sample. Sediment samples (1 cm depth) were
    taken with a metal 10-cc core bi-weekly for the first two months and monthly for the last three
    months until the end of the study. The samples were sieved, processed, and analyzed under a
    stereomicroscope to determine the types of species, the number of living vs. dead, and normal vs.
    deformed populations. Preliminary results from the first study season suggest that the oil impacted at
    least one particular species offorams.,Miliaminajusca, resulting in a high percentage of structural
    deformity in comparison to non-oiled specimens. Time-series studies can prove an estimate of the
    time required for natural attenuation or remedial treatments to reverse this biological effect.

2.2.5.1.3  Bioassays. Establishing the actual exposure level of biota to residual oil is difficult. While
chemical measures of oil in sediments, water, and tissues are routine, there is no guarantee that all
biological organisms accumulate oil or its components equally or in proportion to environmental
concentrations. Further, many of the components of oil such as alkanes and PAHs are metabolized,
so that chemical analyses of tissue may not represent the true dose or dose rate. The key to sediment
assessment is bioavailability since elevated concentrations of toxic compounds may not necessarily
result in adverse effects to the organisms living within the sediments. The only means of measuring
bioavailability is by measuring or determining biological response. Such testing has often involved
measures of bioaccumulation (the ability of an organism to accumulate contaminants in tissues).
However, because bioaccumulation is a phenomenon, not an effect (and can be relatively expensive
to determine due to costly chemical analyses), emphasis has shifted towards indicative endpoints
that are based on sediment toxicity tests, which are effects-based and relatively inexpensive.

•   Microtox solid phase test. In the Microtox® Solid Phase Test (AZUR Environmental, 1999; Lee et
    a/., 1995b; Microbics Corporation, 1992), the bacterium, Vibriofisheri, is exposed to test sediments.
    A significant decrease in bioluminescence relative to water-only controls is indicative of sediment
    toxicity. Toxicity levels are calculated as the concentration of sample that would result in a 50%
    reduction in luminescence ('effective concentration,' ECso). To account for interference from
    differences in sample grain size distribution, turbidity, and to a lesser extent, color  of the sample
    dilutions, sample test results were compared with results from unoiled sediments from  the
    immediate study area.

    Oil toxicity was evident on comparison of oiled with unoiled plots (Figure 2.5a). If one sets an
    arbitrary ECso toxicity threshold at 1,000 mg/L [which Environment Canada uses in its regulations
    (Tay et a/., 1997)], then even though there was a detrimental response observed in the control
    sediments treated with nutrients only, all unoiled sediment samples would be deemed non-toxic
    according to this guideline, while toxicity was identified following oil treatments (Fig. 2.5a). There
    is no implied suggestion that the 1,000 mg/L threshold is being or should be adopted by EPA. The
    threshold was reported as an example to demonstrate how one may utilize toxicity data in decision-
    making. On comparison of results, it appears that natural attenuation (the bars labeled Oil in the
    figure) could account for most recovery. By week 9, all treatments were non-toxic. The significance
    of natural attenuation was also illustrated by a comparison of the relative recovery of the plots using
    ECso's for each treatment and sampling time normalized to the unoiled control (Fig. 2.5b).
                                            40

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Control Nf°ntro'
Nutrients

Oil

Oil
Nutrients


Oil Oil
Nutrients Nutrients
Cut Disking
Figure 2.5. Sediment toxicity for sediment samples from Conrod' s Beach, Nova Scotia, at weeks 0
to 62, as reflected by (a) EC50 for experimental treatments and (b) EC50 normalized to the mean
control value at each sampling time. Error bars =  1 standard deviation.
                                            41

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   Amphipod survival test. The Amphipod Test measured the effects of sediment samples on survival
   of sediment-dwelling Eohaustorius estuarius (Environment Canada, 1992). Both the mean percent
   survival and the mean weight of animals in each treatment were compared with mean percent
   survival and mean weight of amphipods in reference control sediments to determine if the treatments
   caused a significant decrease in organism survival or growth. The results are reported as percent
   mortality (Figure 2.6). Mortality was high in all of the oiled treatments, but it began to decrease by
   Week 12 largely as the result of natural processes. Addition of nutrients accompanied by disking
   appeared to cause the most rapid rates of detoxification (recovery) within the oiled plots as measured
   by this test. However, the results of chemical analyses (GC/MS) indicated that this observation
   could also be attributed to the physical removal of oil (enhanced dispersion with tides) mediated by
   disking operations. By Week 62, the difference between the disked plots and the natural attenuation
   plots was highly significant (32% vs. 5% mortality).



^
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100
90
80
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Figure 2.
Survival
                                                  1
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               Control
                   Control
                   Nutrients
                                          Oil
6.
Test
                                       Oil          Oil           Oil
                                    Nutrients    Nutrients     Nutrients
                                                   Cut        Disking
Changes in sediment toxicity from 0 to 62 weeks as quantified by the Amphipod
Error bars = 1 standard deviation
    Gastropod survival. Although many organisms have been used as sentinels or bio-monitors of
    environmental contaminants (LeBlanc and Bain, 1997), there is still a need to identify and exploit
    alternative species that are sensitive and amenable to ecotoxicological testing. Mollusks are
                                             42

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abundant and widely distributed, and their use as in situ bio-monitors has been on the rise (Lagadic
and Caquet, 1998). Saltwater marshlands present unique restoration challenges following oil spills
due to the sediment's high capacity for oil absorption, low oxygen content, fluctuating salinity, and
tidal flow. The mud-snail, Ilyanassa obsoletci, an abundant detritovore inhabiting these marshlands,
was  evaluated for  its  suitability as  a bio-monitor to assess the impacts or efficacy  of the
bioremediation treatments. It was selected for use as an in situ bio-monitor as it feeds on sediment
detritus, algae and decaying organic matter within the wetland. Snails (n = 50/treatment/sampling
time) were caged in 20 x 20 x 22 cm open mesh polypropylene baskets moored to the sediment
surface of experimental plots. At the end of the second year, cages were recovered after being
exposed to the experimental plots for 30,60 and 90 days to evaluate effects on survival at the end of
the second field season (Week 62). Healthy snails were also exposed for a 30-day period under
laboratory conditions to test sediments recovered from the plots, and to determine survival rates. The
mud snails did not survive long in captivity in the field, and laboratory exposures were  erratic.
Mortality in the field was likely due to environmental factors as mortality was high even in control
cages. It is unlikely that anoxia due to crowding and/or eutrophic conditions was a factor since these
snails are tolerant of anoxic conditions and can grow in dense aggregates. Mortality after 5 d
exposure was generally higher for snails caged within the experimental plots amended  with
nutrients. This toxic response was attributed directly to the use of fertilizers.

Acute and chronic effects on fish. Fish biotests were performed with salt marsh sediments recovered
from the experimental site at Conrod's Beach, Dartmouth, Nova Scotia using euryhaline rainbow
trout. Bioavailability was assessed by quantifying the extent of CYP1A (MFO enzyme, see Section
1.3.5.2) induction (Guiney et a/.,  1997) in  fingerling trout following 96 h  exposures  to test
sediments.   S-9  fractions from  liver homogenates were prepared for the measurement  of
ethoxyresorufin-o-deethylase  (EROD, CYP1A  enzyme)  activity (Hodson et a/., 1996). Each
bioassay included negative controls (water only), un-oiled sediment controls, and positive water
controls  (fish  exposed  to the  compound  B-naphthoflavone,  which  is  a model inducer).

All data were analyzed after log transformation and the extent of induction  calculated by
normalizing to control activity, i.e. induction equaled activity of treated fish divided by activity of
control fish, and hence had no units. The Mesa crude oil contained sufficient PAH to cause high
levels of EROD induction in trout, as shown by a preliminary bioassay of clean sediments spiked
with oil in the lab (10 mL oil/L of sediment). By diluting the spiked sediment with clean sediment, a
clear exposure-dependent gradient of induction was found (Figure 2.7). The plateau of activity at the
highest oil concentrations suggests acute toxicity (Hodson etal.  1996), likely due to the combined
narcotic effects of all the components of oil. A similar effect was observed when oil was  simply
added to water (data not shown). The threshold concentration causing induction was about 0.1 mL
oil/L of reference sediment (Figure 2.7).
                                         43

-------
             100
I
         o
         &
         O
         o
         a:
         LU
              10 -
              0.1
                 0.1                           1
                         Oil Concentration (mL/L sediment)
                                                                  10
Figure 2.7.  EROD activity of rainbow trout exposed to reference sediments spiked with oil. Error
bars are 95% confidence limits while the shaded zone represents the 95% confidence limits of
control activity. Numbers represent sample sizes.

Study results showed that PAHs were bioavailable from Conrod's Beach oiled sediments. While
EROD induction was evident for fish exposed to sediments sampled  1 d after oiling, induction
actually increased in July (50 d later) before decreasing somewhat in October (140 d; Figure 2.8).
The initial  low extent of induction may have  been caused by oil  toxicity.  With higher oil
concentrations, it is likely that EROD induction was inhibited, as was evident from the leveling-off
of the exposure-response curve in the test of sediments spiked with oil in the lab (Figure 2.7). There
did not appear to be a major effect of bioremediation treatments, with the possible exception of
disking. Plots disked to aerate the sediment showed 45% lower EROD induction potency (p<0.05)
than plots with or without nutrients (Figure  2.9). The plots with plants cut showed 44% lower
induction potency, but the difference was just below the level of statistical significance. Disking may
have reduced induction potency by facilitating the transport of oiled surface sediments into deeper
underlying  sediments, enhancing the dispersion of disturbed surface sediments  by tides, and
stimulating microbial activity by improving oxygen availability within the wetland sediments (Lee
2000b).
                                          44

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                          100  H
                      c
                      o
                      D
                     "D
                     _C
                     Q
                     O
                     tE
                     HI
         10  -
                                0            100         200
                                      Days fro m oiling
Figure 2.8. MFO induction in fish exposed to oiled sediments. Each point is the average of data
pooled across all treatments. Error bars = 95% confidence limits. Numbers = sample size.
                  100i
                 c
                 o
                 is
                 D
                 •o
                Q
                O
10-
                    1 -
                   0.1
     *       *
    JJ
                      Control  Control    Oil      Oil       Oil      Oil
                             Nutrients         Nutrients   Nutrients  Nutrients
                                                       Cut     Disking

Figure 2.9. Effect of experimental treatments on EROD induction of trout exposed to oiled
sediments. Asterisk indicates induction was significantly lower than the highest activity. Error bars =
95% confidence limits. N = 15/treatment.

In summary, because there was a strong link between concentrations of PAHs in beach sediments
and the extent of induction in exposed trout, the induction bioassay successfully tracked the changes
over time in the concentrations and bioavailability of PAH and of the crude oil itself. Over the long
term, we would expect that the relationship between induction and uptake of non-PAH hydrocarbons
would weaken due to the differential rates of degradation and weathering of different components of
oil. However, within the time frame of this study, it appears that both the bioremediation and
phytoremediation treatments did not markedly affect the rate of PAH degradation. While there
appeared to be a significantly greater loss of PAH from aerated sediments, the overall enhancement
was less than two-fold, which is at the limit of detection of the induction bioassay for the sample
sizes tested.
                                          45

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Preliminary studies with eyed-eggs (about 15 d post fertilization) of trout also suggested that
symptoms  of Blue  sac  disease  (BSD - characterized  by yolk  sac  and pericardial  edema,
hemorrhaging, deformities, and induction of mixed function  oxygenase enzymes) were  more
frequent in fish exposed to oiled than to un-oiled sediments (Zambon etal., 2000); indicating a risk
to early life stages of species that spawn on tidal beaches.

These laboratory bioassays with fish represent a 'worst-case' scenario as the test organisms could
not avoid exposure to sediments that have been mixed, thereby destroying surface layers that might
be depleted of oil due to weathering. The ratio of water to sediment was also fixed, which is very
different from the situation in well-flushed tidal beaches. Finally, the test species is a useful model,
but is not a beach spawner. Nevertheless, the model fish do provide a useful surrogate for  other
species, such as smelt, capelin, and herring that spawn on both freshwater and marine beaches or in
marine littoral zones. In many estuaries, contaminated water is often not well mixed, but moves back
and forth with the tide, thereby causing prolonged exposure of fish entrained in the water  mass
(Elson et al.  1972).  As illustrated by the Exxon Valdez spill, eggs deposited in beach sediments
cannot move and are also subject to continuous exposure. The utility of freshwater species as a
surrogate for marine species might also be questioned. However, it is worth noting that eggs of pink
salmon, a species closely related to rainbow trout, were  exposed to oil from the Exxon Valdez
because they were spawned in river mouth shoals (Marty et al.  1997). The  eggs were bathed
alternately  in fresh and salt water as the tide rose and fell, so that an exposure  of trout to  oiled
sediments in saline water is not entirely unrealistic. To resolve the uncertainties associated with
assessing exposure and effects, it is clear that the next step is  to refine and adapt bioassays for
application in situ, using species endemic to the test sites.

2.2.5.2 Risk assessment

In this case study, overall sediment quality was determined from the integration of results  from
analysis of sediment chemistry, community structure, alteration of primary metabolic processes, and
sediment toxicity. The  results of detailed chemical analysis, bioassessments, and bioassay tests
suggested that in the Conrod Beach study, natural attenuation was the primary process that reduced
residual oil concentrations and toxic effects.  The biotest results showed that  the remediation
strategies under evaluation, stimulation of bioremediation and phytoremediation activity by nutrient
amendments and physical mixing (disking), were not highly effective in regards  to restoration. It
was also evident in the  results of some biotests (e.g. Amphipod Survival Test, Microtox Test) that
possible detrimental effects may be linked to the addition of fertilizers.

It is imperative that one fully understands the various processes that may affect biotest endpoints.
Failure of the Gastropod Survival Test to resolve differences in experimental treatments could be
attributed to adverse environmental conditions that caused high levels of inherent variability within
the test matrix. The Biotox Solid-Phase Flash Assay (Lappalainen et al, 1999) is currently being
considered as a relevant  adjunct (or alternative) test  to the Microtox solid-phase assay, since it
allows the evaluation of large numbers of environmental samples at a more reasonable cost using the
same test organism. This assay was used with success to provide evidence of toxicity reduction by
remedial activities in an oil-impacted freshwater environment (Blaise et al., 2002).  However, in this
case study, all sediments collected during the first 2 sampling events (Week 0,2) show marked and
                                           46

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similar levels of toxicity. It is hypothesized that the assay was unable to discriminate between
toxicity of oiled and unoiled sediments, as it was responding to the presence of natural contaminants
present in the anaerobic sediments (e.g., NH3 and/or H2S) and possibly also to their degree of oil
contamination (in the case of the  oiled sediments). Similarly, the Algal Toxicity Test with
Selenastrum capricornutum (Blaise and Menard, 1998) that readily identified the inhibitory effects
of residual oil in sediments on esterase enzyme activity in the previous freshwater marsh case study
was ineffective in this test case. This was attributed to interferences associated with benthic diatom
growth. This has necessitated the development of a new algal toxicity test using the marine macro-
alga Champiaparvula to assess archived sediments from this study.

With further refinement, guidelines for  selection of bioassessment and bioassay test suites will be
provided to oil spill  response managers that are tasked to implement and verify the success of
countermeasure operations including the extent of habitat recovery. For this case study in a marine
salt marsh environment, the results of the ecological risk assessment with all available  quantitative
chemical and biological data suggest that natural attenuation may be the most environmentally sound
and cost-effective treatment option. Although there was some evidence of changes in microbial
community structure  and activity, no significant differences were observed among treatments in oil
degradation rates or toxicity reduction. Active remedial treatment is not supported by cost-to-benefit
analyses.

2.3   Summary and Recommendations

Most of the information presented in this guidance document was based on only a few field studies
of oil bioremediation. Not many studies have been done in a definitive manner. The Conrod Beach
experiment in Dartmouth, Nova Scotia, demonstrated that biodegradation of the alkane  fraction and
some of the PAH fraction was stimulated following the application of inorganic fertilizers directly to
the plots. Disking (or tilling) caused substantial damage to  the rhizosphere, and such drastic
measures cannot be recommended as a  means of increasing oxygen content in  the root zone. Not
much can be done in that regard. Thus, if significant penetration has taken place into the subsurface,
then not  much hope of acceleration in hydrocarbon disappearance is possible since anaerobic
conditions rapidly set in at greater depths. If, however, penetration is limited to the top several mm,
then sufficient oxygen might be available to permit biostimulation to accelerate greater hydrocarbon
disappearance than via natural attenuation. So, of major importance in the event of an  oil spill in a
salt marsh (or any wetland oil spill) is to assess the degree to which penetration has  taken place
below the surface. If it is minor, then biostimulation could be  considered as a viable  strategy for
cleanup.  If it is more than a few  mm penetration, then biostimulation will have  diminished
effectiveness due to the increased likelihood of limiting oxygen concentration in the oil impact zone.

Salt marshes are among the most sensitive ecosystems and, therefore, the most difficult to clean.
Applications of some traditional oil spill cleanup techniques in wetland habitats have caused more
damage than the oil itself. Several long-term field studies have been carried out in coastal wetlands
to evaluate the potential of oil bioremediation, one of the least  intrusive technologies.  The studies
have shown that oil biodegradation on  coastal wetlands is often limited by oxygen,  not nutrient
availability. Natural attenuation is increasingly becoming the preferred strategy for the restoration of
oil-contaminated wetlands. However, field studies also indicate that nutrient amendments may still
be a viable option for removing hydrocarbons from an oil-contaminated wetland if the oil does not
                                           47

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penetrate deeply into the anoxic zone of wetland sediments and when nutrients are limiting. When
biostimulation is selected, it is recommended that nitrogen concentrations of at least 2 to as much as
10 mg N/L should be maintained in the pore water to achieved optimal oil biodegradation, with the
decision on higher concentrations to be based on a broader analysis of cost, environmental impact,
and practicality. The overall success of the remedial  operations should be not only based on the
efficiency of oil degradation but also the integration  of results from a suite of assays, which are
chosen on  the basis of ecological relevance to the site of concern, cost considerations, and the
availability of technical expertise.
                                            48

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