-------
-Analysis. Report Averages
Ned 10-08-97 00:54:19 AH page 13
Method: TRIANGL2 Sample Nane: ICB/CC8 Operator: DKH
Run Time: 10/07/97 04:19 Filenaae: 100797
Mode: CONC _ Type: Q Corr. Factor: 1.00000
Lab ID.: Cust. Soph ID.: Cust. ID.: 43430
El eras
Units
Avge
SDev
%RSO
Elems
Units
Avge
SDev
*RSD
El eras
Units
Avge
SDev
*RSD
Elems
Units
Avge
SDev
iRSO
Elems
Units
Avge
SDev
%RSD
Ag3280
ppb
.1153
.3559
308.6
A1308
ppb
35.78
3.024
8.4-52
ppb
-.7492
1.582
211.1
ppb
-208.7
.9138
.4379
Cr2677 Cu3247
ppb ppb
.1302 -1.267
.1114 .1472
85.5 11.61
C64186
ppb
-.4512
.5508
122.1
Mn2576 No2020
ppb ppb
.0309 .1208
.018 .3677
58.21 304.4
Mg2790
ppb
2.520
.8062
32
2203-2 Sb2068
PPb ppb
-3.434 -.0020
.9822 1.274
28.6 64910
P.2149
ppb
6.483
3.62
55.34
2203-1
ppb
1.209
1.094
90.48
1960-2
PPb
-2.974
2.35
79.02
Snl899
ppb
Q33.02
9.284
28.11
Pb2203
ppb
-1.
.5263
27.88
Sel960
ppb
-1.021
.0971
9.513
Ca3179 Cd2265
ppb ppb
-3.147 -.1175
.6507 .1615
20.68 137.4
Fe2714 K.7664
ppb ppio
2.283 .0175
.6559 .0108
28.72 61.5
Na3302 Ni23
ppn ppb
.0545 yC0893
.0629 /276
115.4 /366.8
101V/
Elems
Units
Avge
SDev
*RSD
Ti3J49
ppb \
-.0190
.066
348.2
T11908
smb ._
Q5.048
2.915
57.75
V.2924
ppb -
1.557
.3821
24.54
Zn2062
— PP»
.1679
.1562
93.01
.SJ2881
~~PPi>
Q-628.5
.091
.0145
206
-------
"halysisJSport Averages • Wed 10-08-97 00:5*4:19 AM page 14
nethod: TRIAHGL2 Saaple Naae: IC8/CCB Operator: DKH
iun Tine: 10/07/97 04:31 Filename: 100797
riode: CONC Type: Q Corr. Factor: 1.00000
Lab ID.: Cust. Snpl. ID.: Cust. ID.: 43430
Elems
Inits
*vge
SOev
IRSD
Elenis
Units
4vge
SOev
$RSD
Elems
Units
Avge
SOev
*RSD
Elems
Units
Avge
SDev
*RSD
Elems
Units
Avge
SDev
%RSD
El ens
Units
Avge
SDev
*RSD
Ag3280
ppb
.1661
.1269
76.43
Ca3179
ppb
-4.096
.5473
13.36
Fe2714
ppbi
3.309
3.475
105
Na3302
ppni
.0360
.1033
302.3
1960-1
ppb
2.833
1.608
56.76
Ti3349
ppb
-.0126
.061
482.6
A13082
ppb
40.81
2.658
6.514
Cd2265
ppb
-.0758
.018
23.78
KJ664
ppoi
.0201
.012
59.67
Ni2316
ppb
-.0023
.6983
29790
1960-2
ppb
-.9544
1.044
109.4
T11908
ppb
3.302
2.898
87.78
AS1390
ppb
1.251
.9621
76.89
CB4186
ppb
.1982
.5162
260.5
Li6707
ppb
.0755
.0337
44.56
PJ149
ppb
3.424
1.303
38.06
Pb2203
ppb
-.9020
.276
30.6
V.2924
ppb
1.671
.386
23.09
8.2496
ppb
-211.7
1.69
.7981
C02286
ppb
.0802
.3625
451.9
Mg2790
ppb
.5514
3.487
632.4
2203-1
ppb
.8929
1.807
202.4
Sel960
ppb
.3063
.9219
300.5
Zn2062
ppb
.1510
.3774
249.9
Ba4934
ppb
-.Oltt
.0428
370.3
Cr2677
ppb
.1499
.3166
211.2
Mn2576
ppb
.0024
.0446
1849
2203-2
ppb
-1.798
.9609
53.44
Snl899
ppb
Q13.43
14.7
109.1
.Si2881
ppb
Q-651.2
1.713
.2631
8e3130
ppb
-.2269
.016
7.059
CU3247
ppb
-1.328
.129
9.711
H02020
ppb
-.5559
.2651
47.68
Sb2068
ppb
.3855
1.052
272.9
Sr4215
PPb
-.0077
.0227
294.2
207
-------
Analysis' Report Averages
Sed 10-08-97 00:54:19 Ail page 15
Method: TRIAN6L2 Sample Name: ICSA8 Operator: DXH
Run Time: 10/07/97 04:37 Filename: 100797
Node: CONC Type: Q Corr. Factor: 1.00000
Lab 10.: Cust. Sapl. 10.: Cust. 10.: 43430
Elems
Units
Avge '
SOev
IRSD
Elems
Units
Avge
SOev
IRSO
Elems
Units
Avge
SOev
*RSD
Eleus
Units
Avge
SOev
*RSD
Elems
Units
Avge
SDev
%RSD
Elems
Units
Avge
SDev
*RSO
Ag3280
ppb
531.9
1.237
.2325
Ca3179
ppb
448500.
1338
.2983
Fe2714
ppb
172700.
245.2
.142
Na3302
ppg
5.589
.0987
1.766
1960-1
ppb
537.0
7.339
1.367
Ti3349
ppb
499.6
.3489
.0698
A13082
ppb
501000.
3412
.6809
Cd2265
ppb
480.7
1.042
.2168
K.7664
PPB
025.34
.1569
.6191
Hi2316
ppb
462.5
1.248
.2699
1960-2
ppb
527.6
7.309
1.385
T11908
PPb
503.0
23.13
4.598
AS1890
ppb
522.8
4.091
.7826
Ce4186
ppb"
504.2
1.044
.2071
Li6707
ppb
625.0
3.643
.5823
P.2149
ppb
545.5
12.9
2.365
Pb2203
ppb
488.3
1.6
.3277
V.2924
ppb
493.6
1.132
.2294
8J496
ppb
324.4
3.635
1.121 _.
C02286
ppb
470.5
1.251
.2659
Hg2790
ppb
527500.
598.2
.1134
2203-1
ppb
491.5
5.464
1.116
SS1960
ppb
530.7
2.762
.5203
Zn2062
ppb
446.6
3.533
.7911
834934
ppb
518.5-
1.233
.2378
Cr2677
ppb
480.2
2.242
.467
Hn2576
ppb
459.9
1.24
.2696
2203-2
ppb
486.6
5.071
1.042
Snl899
ppb
Q9712.
111.3
1.146
.Si288i
ppb
Q-63.97
5.421
8.475
8e3130
ppb
482.5
1.742
.361
Cu3247
ppb
542.6
3.815
.7031
M02020
ppb
496.5
4.086
.8231
Sb2068
ppb
510.1
3.386
.6637
Sr4215
ppb
512.5
.9922
.1936
208
-------
Analysis Report Averages
Bed 10-08-97 00:59:04 AN page 1
Method: TRIANGL2 Sample Name: 43231 MB Operator: DKH
Run Tine: 10/07/97 05:09 Filenaue: 100797
Mode: CONC Type: S Corr. Factor: 1.00000
Lab ID.: Cust. Snipl. 10.: Cust. ID.: 43231
El ems
Units
Avge
SDev
tRSD
Co2286 Asl890 6a4934 Be3130 Cd2265 Ag3280
ppb ppb ppb ppb ppb ppb
L-.0840 L.2054 L.1336 1.3012 L-.1924 1.0129
.0786 1.789 .023 .0141 .036 .1976
93.54 870.9 17.21 4.686 18.73 1535
Elems
Units
Avga
SOev
%RSD
Cr2677
ppb
L.2336
.2472
105.8
Mn2576
ppb
L.8014
.057
7.111
IU2316
PPb"
L.7729
.5292
68.46
P.2149
ppb
L3.209
1.384
43.14
Pb2203
ppb
L-.0667
.3606
540.9
Sb2068
ppb
L.4985
.7593
152.3
El 80S
Units
Avge
SOev
%RSD
Sel960
ppb
L.0967
2.06
2129
T11908
ppb
L3.807
1.589
41.72
Zn2062
ppb
22.53
.2129
.9451
209
-------
:Analysis Report • Averages
Bed 10-08*97 00:59:04 AH page 2
Method: TRIAN6L2 Sample Name: 43231 LCS Operator: OKH
Run Tine: 10/07/97 05:14 Filename: 100797
Node: CONC Type: S Corr. Factor: 1.00000
Lab ID.: Oust. Sapl. ID.: Cust. ID.: 43231
Eleois
Units
Avge
SDev
IRSD
C02286
ppb
49.51
.4746
.9586
AS1890
ppb
49.55
1.37
2.766
Ba4934
ppb
50.04
.0505
.101
Be3130
ppb
47.96
.0718
.1496
Cd2265
ppb
50.41
.2798
.5543
Ag3280
ppb
46.92
.4211
.8974
Eleins
Units
Avge
SDev
IRSD
Cr2677 Mn2576
ppb ppb
50.38 50.22
.5406 .1382
1.073 .2751
N12516
PPb'
50.80
.9832
1.936
P_2149
ppb
1027.
9.016
.8777
Pb2203 Sb2068
ppb ppb
48.37 51.11
.2561 .9948
.5295 1.947
Elems
Units
Avge
SDev
%RSO
Sel960
ppb
48.39
.8738
1.787
T11908
ppb
54.98
.8596
1.563
Zn2062
ppb
202.1
.9752
.4825
210
-------
Analysis Report Averages
Wed 10-08-97 00:59:04 AN page 3
Method: TRIANGL2 Sample Name: 183-3-18 Operator: DKH
Run Tine: 10/07/97 05:19 Filenaae: 100797
Mode: CONC Type: S Corr. Factor: 1.00000
Lab ID.: Cust. Snpl. ID.: Cust. ID.: 43231
Elems
Units
Avge
SDev
*RSD
Co2286
ppb
L-1.503
.2874
19.12
AS1890
ppb
L2.984
1.066
35.71
Ba4934
ppb
4.282
.0153
.3576
8e3130
ppb
L.2732
.0461
16.9
Cd2265
ppb
25.20
.185
.7342
Ag3280
ppb
5.430
.3719
6.85
Elems
Units
Avge
SDev
IRSD
Cr2677 Mn2576 Ni2316 P.2149 Pb2203 Sb2068
ppb ppb ppb' ppb ppb ppb
9.808 7.089 9.264 L19.49 134.9 6.088
.3586 .0144 .4954 4.19 1.735 1.037
3.657 .2033 5.348 21.5 1.286 17.04
Eleas
Units
Avge
SDev
%RSD
Sel960
ppb
3.900
2.003
51.35
T11908
ppb
L-.5224
1.752
335.5
Zn2062
Ppb
42.38
.3113
.7356
211
-------
analysis Report Averages
Wed 10-08-97 00:59:04 AH page 4
Method: TRIANGL2 Sample Name: 183-3-2B Operator: DKH
Run Time: 10/07/97 05:23 Filename: 100797
Mode: CONC Type: S Corr. Factor: 1.00000
Lab ID.: Cust. Srapl. ID.: Cust. ID.: 43231
Eleias
Units
Avge
SDev
IRSD
C02286 AS1890 8a4934 8e3130 M2265 Ag3280
ppb ppb ppb ppb ppb ppb
1-1.725 7.435 51.46 L.3328 28.57 10.58
.43 1.497 .0976 .0402 .2591 .6289
24.92 20.13 .1896 12.08 .9066 5.946
Eleras
Units
Avge
SDev
USD
Cr2677
PPb
41.40
2.048
4.946
Mn2576
ppb
1584.
8.431
.5321
Ni2316
PPb"
50.42
1.657
3.287
PJ149
ppb
105.6
5.198
4.924
Pb2203
ppb .
1914.
12.68
.6o25
Sb2068
ppb
23.73
3.3
13.9
Eleois
Units
Avge
SDev
*RSD
Sel960 T11908 Zn2062
ppb ppb ppb
8.559 L-2.244 11380.
1.332 2.784 110.3
15.56 124.1 .9692
212
-------
••Analysis Report Averages
Ned 10-08-9? 00:59:04 AM page 5
Method: TRIANGL2 Sample Nane: 183-3-28 PDS Operator: DKH
ton Time: 10/07/97 05:28 Filename: 100797
lode: COHC Type: S Corr. Factor: 1.00000
Lab ID.: Cust. Snpl. ID.: Cust. ID.: 43231
Elens
Units
4vge
SDev
%RSD
Co2286
ppb
46.53
.3865
.8308
Asl890
ppb
52.32
1.785 •
3.411
8a4934
ppb
100.9
.3536
.3505
8e3130
ppb
45.60
.1294
.2837
Cd2265
ppb
77.08
.5125
.6649
Ag3280
PPb
56.28
.5567
.9892
Elens
Units
Avge
SOev
%R5D
Cr2677
ppb
91.75
1.525
1.662
Hn2576
ppb
1619.
5.874
.3628
Ni2316
ppb'
99.32
1.766
1.778
P.2149
PPb
106.6
12.33
11.56
Pb2203
ppb
1945.
7.356
.4039
Sb2063
ppb
68.97
1.48
2.145
Elems
Units
Avge
SDev
USD
Sel960 T11908 2n2062
ppb ppb ppb
53.34 46.28 11470.
.2419 2.999 98.47
.4534 6.479 .3534
213
-------
: Analysis Report Averages fled 10-08-97 00:59:04 AN page 6
Method: TRIAN6L2 Sample Name: 183-3-28 I Operator: DKH
Run Time: 10/07/97 05:33 Filenaoe: 100797
Mode: CONC Type: S Corr. Factor: 1.00000
Lab ID.: Cust. Smpl. ID.: Cust. ID.: 43231
Elems
Units
Avge
SDev
4RSD
Co2286 Asl890 8a4934 8e3130 Cd2265 Ag3280
ppb ppb ppb ppb ppb ppb
L-1.100 L2.140 10.54 L.3221 5.654 2.246
.1214 1.787 .063 .0306 .161 .3491
11.03 83.51 .598 9.491 2.846 15.54
Elens Cr2677 Mn2576 Ni2316 PJ149 Pb2203 Sb2068
Units ppb ppb ppb' ppb ppb ppb
Avge 12.65 327.6 12.88 31.59 402.2 8.209
SDev .3954 .7695 .337 8.045 2.606 1.123
IRSD 3.127 .2349 2.616 25.47 .6479 13.68
Elens
Units
Avge
SDev
%RSD
Sel960
ppb
3.531
1.877
53.16
T11908
ppb
13.416
2.182
63.87
Zn2062
PPb
2410.
3.5r>3
.3556
214
-------
-.Analysis Report Averages
Wed 10-08-97 00:59:04 AM page 7
Method: TRIAN6L2 Sample Name: 183-3-3B Operator: DKH
Run Tine: 10/07/97 05:37 Filenaie: 100797
Mode: CONC Type: S Corr. Factor: 1.00000
Lab ID.: Cust. Smpl. ID.: Cust. ID.: 43231
Eleias
Units
Avge
SDev
%RSD
Co2286 Asl890 8a4934 Be3130 Cd2265 Ag3280
ppb ppb ppb ppb ppb ppb
5.101 29.56 272.5 1.477 298.9, 50.48
.1027 1.621 .1511 .0157 .7584 .4574
2.014 5.483 .0555 1.065 .2537 .9062
Elems
Units
Avge
SDev
%RSD
Cr2677
ppb
154.5
1.403
.9083
Mn2576
ppb
12560.
18.43
.1468
N12316
ppb-
51.42
1.221
2.375
P.2149
ppb
420.2
8.107
1.929
PD2203
ppb
14900.
8.949
.0601
Sb2068
ppb
105.9
2.9
2.739
El ems
Units
Avge
SDev
%RSD
Sel960
ppb
18.31
1.038
5.516
T11908
ppb
14.67
.9247
6.302
Zn2062
ppb
H72520.
206.2
.2843
215
-------
Analysis Report Averages
Ned 10-08-97 00:59:04 AM
page 8
Method: TRIANGL2 Sample Name: 183-3-38 DA Operator: DKH
Run Tine: 10/07/97 05:42 Filename: 100797
Mode: CONC Type: S Corr. Factor: 1.00000
Lab ID.: Cust. Smpl. ID.: Cust. ID.: 43231
El ens
Units
Avge
SDev
*RSD
C02286
ppb
4.991
.3913
7.84
Asl390
ppb
33.61
2.12
6.307
8a4934
ppb
273.6
.2217
.081
8e3130
ppb
1.475
.0297
2.015
Cd2265
ppb
298.8
1.402
.4691
Ag3280
ppb
50.49
.2812
.5569
El eras
Units
Avge
SDev
*RSD
Cr2677
ppb
155.2
1.801
1.16
Hn2576
ppb
12520.
56.51
.4514
Ni2316
PPb"
52.03
.4253
.8174
P.2149
ppb
425.2
2.365
.5562
Pb2203
ppb
14910.
58.42
.3919
Sb2068
ppb
106.9
1.539
1.44
Eleios
Units
Avge
SDev
%RSD
Sel960
ppb
18.29
1.813
9.938
111908
ppb
13.08
3.168
24.21
Zn2062
ppb
H71960.
469.5
.6525
216
-------
•'Analysis Report Averages
Ned 10-08-97 00:59:04 AM page 9
Method: TRIANGL2 Sample Name: 183-3-48 Operator: DKH
Run Time: 10/07/97 05:47 Filenaue: 100797
Mode: CONC Type: S Corr. Factor: 1.00000
Lab ID.: Cust. Stipl. ID.: Cust. ID.: 43231
Hems
Units
Avge
SDev
USD
C02286
ppb
L-1.676
.4468
26.66
AS1890
ppb
8.563
1.731
20.22
8a4934
ppb
48.03
.2026
.4218
Be3130
ppb
L.4056
.0434
10.69
Cd2265
ppb
25.08
.1776
.7083
Ag3280
ppb
7.181
.3424
4.768
El ems
Units
Avge
SDev
*RSD
Cr2677
ppb
30.49
1.071
3.514
Mn2576
ppb
1505.
5.021
.3338
Ni2316
ppb'
13.72
.9878
7.201
P.2149
ppb
1565.
1.35
.0863
P62203
ppb
1491.
4.75
.3186
Sb2068
ppb
14.70
2.254
15.33
El ems
Units
Avge
SDev
%RSD
Sel960
ppo
8.715
1.429
16.4
T11908
PPb
L-1.443
4.736
328.2
Zn2062
ppb
3545.
72.11
.3439
217
-------
.Analysis- Report Averages
Bed 10-08-97 00:59:04 AM page 10
Method: TRIANGL2 Sample Name: 183-3-58 Operator: DKH
Run Time: 10/07/97 05:51 Filename: 100797
Mode: CONC Type: S Corr. Factor: 1.00000
Lab ID.: Cust. Snpl. ID.: Cust. ID.: 43231
El ems
Units
Avge
SDev
IRSD
Co2286 Asl890 Ba4934 8e3130 Cd2265 Ag3280
ppb ppb ppb ppb ppb ppb
L-2.223 L4.119 2.195 L.2215 L-.1931 L.4694
.4794 1.927 .0116 .0272 .0138 .1325
21.57 46.79 .53 12.29 7.125 28.24
Elems
Units
Avge
SDev
SRSO
Cr2677 Mn2576 Ni2316 PJ149 Pb2203 Sb2068
ppb ppb ppb' ppb ppb ppb
10.44 11.41 6.462 113.13 9.729 7.605
.9226 2.011 1.026 4.668 3.117 2.898
8.84 17.63 15.87 35.57 32.04 38.11
Elems
Units
Avge
SDev
SRSD
TH903 Zn2062
ppb ppb ppb
6.198 Ll.619 61.34
2.272 i.43 12.74
36.65 88.36 20.78
21S
-------
Analysis Report Averages
Ned 10-08-97 00:59:04 AM page 11
Method: TRIAN6L2 Sample Naae: ICV/CCV Operator: OKH
Run Tine: 10/07/97 05:57 Filename: 100797
Mode: CONC Type: 0 Corr. Factor: 1.00000
Lab ID.: Cust. Snpl. ID.: Cust. ID.: 43231
El ems
Units
Avge
SDev
%RSD
Elems
Units
Avge
SOev
*RSD
Elems
Units
Avge
SDev
*RSD
Elems
Units
Avge
SDev
*RSD
Elems
Units
Avge
SDev
*RSD
Elens
Units
Avge
SDev
*RSD
Ag3280
ppb
500.1
1.768
.3536
Ca3179
ppb
496.2
1.349
.2717
Fe27l4
ppb
504.5
2.803
.5557
Na3302
ppm
4.790
.0763
1.593
1960-1
ppb
494.3
5.34
1.08
H3349
ppb
500.4
.8618
.1722
A13082
ppb
549.8
11.63
2.116
Cd2265
ppb
506.5
2.453
.4844
X_7664
ppoi
4.770
.0039
.0827
Nil'316
ppb
508.6
1.098
.2159
1960-2
ppb
'SOO.3
2.733
.5556
111903
ppb
501.9
15.59
3.106
AS1890
ppb
503.0
2.658
.5284
C64186
ppb'
502.0
.2835
.0565
Li6707
ppb
471.3
1.514
.3212
P.2H9
ppb
506.4
4.205
.8303
Pb2203
ppb
492.7
.3996
.1826
VJ924
ppb
498.5
1.359
.2727
8.2496
ppb
1126.
289.1
25.63
C02286
ppb
491.1
1.704
.3469
Mg2790
ppb
494.2
n -ino
i.iOO
.4629
2203-1
ppb
477.5
13.53
2.835
Sel960
ppb
493.6
1.65
.331
Zn2062
ppb
495.1
1.921
.3879
8a4934
ppb
499.6
.8604
.1722
Cr2677
ppb
508.3
3.19
.6276
Mn2576
ppb
494.5
1.959
.3962
2203-2
pob
500.3
5.416
1.083
Snl899
ppb
Q9060.
42.96
.4741
Si288l
ppb
Q134400.
14970
11.14
8e3130
ppb
488.5
2.648
.542
Cu3247
ppb
499.3
3.39
.679
«o2020
ppb
495.0
3.113
.629
Sb2Co3
ppb
497.?
2.355
.4729
5r4215
PPb
498.4
.4037
.081
219
-------
•Analysis Report Averages
Bed 10-08-97 00:59:04 AH page 12
Method: TRIANGL2 Sample Name: IC8/CC8 Operator: DKH
Run Time: 10/07/97 06:04 Filename: 100797
Mode: CONC Type: 9 Corr. Factor: 1.00000
Lab 10.: Cust. Srnpl. ID.: Cust. 10.: 43231
Eleios
Units
Avge
SDev
$RSD
Ag3280
ppb
.5385
.2869
53.28
A13082
ppb
Q57.04
2.91
5.101
AS1890
ppb
1.689
.6228
36.87
8_2496
ppb
1103.
345.8
31.34
8a4934
PPb
.2200
.1405
63.37
8e313C
ppb
.5654
.1555
27.49
Elerns Ca3179 Cd2265 Ce4186 _Co22fl6—frf^TJ—Cu3247
Units ppb ppb ppF ppb ppb ppb
Avge -4.869 -.3955 -.7971 -.9458 Q5.127 Q-2.216
SDev .1377 .0709 .4798 .3115 .6631 .4563>
%RSD 2.828 17.94 60.19 32.93 13.03
EleiBS
Units
Avge
SDev
SRSD
Fe2714
ppb
14.13
5.622
39.73
KJ664
ppm
.0282
.0217
77.04
U6707
ppb
.3119
.092
29.51
MQ2790
ppb
i.657/
1.6K
>T56
mut
ufi
' .1839
.1417
77.08
1102020
ppb
.6380
.4317
67.67
El ems
Units
Avge
SDev
IRSO
Ha3302 Ni2316 P.21/9 2203-1 2203-2 Sb2068
ppm ppb MTO ppo ppb poo
.0078 Q3. 213/5. 152 4.331 -5.130 Q4.165
.0636 .587 / 3.26 8.018 3.177 1.559
816.7 18.2i 63.27 166 61.33 37.44
El ems
Units
Avge
SDev
SRSD
1960-1
ppb /
11.58
1.8/S
15/56
/1 960- 2
ppb
-.6711
1.67S
250.1
PD2203
ppb
-1.346
.617
33.42-—
5el?60
ODD
Q3.457
1.174
•ToT'O
Snl399
ppb
g-iG5.i
28.36
27.47
Sr4215
ppb
f\fi^ f
.tLlj
.135
"59.36
Elems
Units
Avge
SDev
$RSD
TJ3349
ppo
.1627
.0632
41.92
T11903
ppb
3.96'}
2.724
68.62
V.2924
ppb
32.349
.2512
10.7
Zfi2062
ppb
1.139
.2836
24.89
Si2351
ppb
Q93760.
11540
12.3
220
-------
'.Analysis Report Averages
Wed 10-08-97 00:59:04 AM page 13
Method: TRIANGL2 Sample Name: ICB/CC8 Operator: DKH
Run Tine: 10/07/97 06:19 Filename: 100797
Mode: CONC Type: Q Corr. Factor: 1,00000
Lab ID.: Cust. Smpl. 10.: Cust. ID.: 43231
Eleits
Units
Avge
SDev
%RSD
Elens
Units
Avge
SOe'v
*RSD
Elems
Units •
Avge
SOev
',RSO
Eleins
Units
Avge
SDev
*RSO
Elens
Units
Avge
SDev
SRSD
Elains
Units
Avge
SDev
*RSD
Ag3280
ppb
-.5317
1.738
326.9
Ca3179
ppb
.5761
.8656
150.2
Fe2714
ppb
5.114
2.113
41.32
Ha3302
ppffl
-.2286
.5526
241.7
1960-1
ppb
4.529
2'. 188
48.31
Ti3349
ppb
.1194
.1123
94.47
A13082
ppb
-.5762
8.903
1545
Cd2265
ppb
.7945
.2941
57.01
KJ664
ppffl
,0601
.0243
40.42 .
Ni2316
ppb
2.343
.1125
4.802
1960-2
ppb
.9633
3.235
334.1
T11908
ppb
Q10.44
1.68
16.09
As 1890
ppb
4.251
.9086
21.37
Ca4136
Ppb'
2.189
1.289
58.91
U6707
ppD
.1608
.0506
31.45
P.2149
ppb
11.40
3.328
29.21
Pb2203
ppb
'l.225
1.312
107.1
V.2924
ppb
Q2.990
.698
23.34
8_2496
ppb
1531.
342.2
22.36
Co2236
Ppb
.2052
.2702 '
131.6
flg2790
ppb
2.086
2.249
107.8
2203-1
ppb
-.3249
3.728
1148
Sel960
ppb
2.154
2.015
93.56
Zn2062
ppb
.6097
.3819
62.65
834934
ppb
.0309.
.0293
94.81
Cr2677
ppo
1.853
.518
27.96
«n2576
ppo
-.0044
.0257
580.7
2205-2
PPb
1.999
3.531
176.7
Snl899
ppb
Q-21.31
17.37
81.52
5i2381
ppb
Q24/30.
9419
38
BeJloO
ppb
.0217
.0526
242.4
CU3247
ppb
Q-2.841
.6563
22.4
H02020
ppb
.1754
.•1378
249.6
3b2065
ppb
1.673
.3552
21.17
Sr4215
PPb
.0393
.0211
54.56
991
^, M» JL
-------
"•Analysis Report Averages
Bed 10-08-97 00:59:04 AM page 14
Method: TRIANGL2 Sample Name: 183-3-6B Operator: DKH
Run Time: 10/07/97 06:24 Filename: 100797
Mode: CONC Type: S Corr. Factor: 1.00000
Lab ID.: Cust. Sgpl. ID.: Cust. ID.: 43231
El eras
Units
Avge
SDev
%RSD
Co2286 AS1890 Ba4934 8e3130 Cd2265 Ag3280
ppb ppb ppb ppb ppb ppb
L-1.806 L4.283 8.844 1.1416 16.44 L.8027
.3095 .36 .0277 .0244 .0362 .5466
17.14 8.406 .3137 17.22 .2201 68.1
Eleiss
Units
Avge
SDev
IRSD
Cr2677
ppb
9.845
.7486
7.604
Mn2576
ppb
29.62
.0633
.2138
Ni2316
PPb"
11.50
.16
1.391
P.2149
ppb
L25.81
2.254
8.734
Pb2203
ppb
241.7
1.067
.4413
Sb2068
ppb
L3.938
1.543
39.19
El eras
Units
Avge
SDev
$RSD
Sel960
ppb
3.725
1.336
49.3
T11908
ppb
L.1661
.2842
171.1
Zn2062
ppb
92.84
.5221
.5624
222
-------
Ana-lysis Report Averages Med 10-08-97 00:59:04 AN page IS
Method: TRIANGL2 Sample Mane: 183-3-7B Operator: DXH
Run Tine: 10/07/97 06:29 Filename: 100797
Node: CONC Type: S Corr. Factor: 1.00000
Lab 10.: Cost. Sipl. ID.: Cust. 10.: 43231
Eleios
Units
Avge
SDev
IRSD
Co2286 AS1890 8a4934 8e3130 Cd226S Ag3280
ppb ppb ppb ppb ppb ppb
L-2.318 5.244 7.222 L.1385 19.51 L.6510
.2215 1.829 .0532 .0252 .0542 .3015
9.553 34.88 .7369 18.16 .2777 46.31
Eleins
Units
Avge
SDev
*RSO
Cr2677
ppb
10.33
.815
7.89
Hn2576
ppb
56.90
.3025
.5317
Ni2316
PPb'
12.71
.6915
5.44
P.2149
ppb
30.66
4.756
15.51
Pb2203
ppb
167.8
.525
.3129
Sb2068
ppb
4.323
1.924
44.5
Eleros
Units
Avge
SDev
%R3D
Sel960 T11908 Zn2062
ppb ppb ppb
4.249 Li. 378 155.9
1.721 .741 1.698
40.51 53.77 1.09
223
-------
. Analysis fteport Averages
Bed 10-08-97 00:59:04 AN page 16
Method: TRIAN6L2 Sample Name: 183-3-88 Operator: DKH
Run Time: 10/07/97 06:34 Filename: 100797
Mode: CONC Type: S Corr. Factor: 1.00000
Lab 10.: Cust. Sipl. 10.: Cust. 10.: 43231
Elens
Units
Avge
SDev
?;RSO
C02286 Asl890 8a4934 Be3130 Cd2265 Ag3280
ppb ppb ppb ppb ppb ppb
L-3.729 5.202 12.50 L.1025 3.949 9.942
.3914 .2739 .1446 .0193 .1164 .1831
10.5 5.265 1.157 18.84 2.948 1.842
Elents
Units
Avge
SDev
%RSD
Cr2677
ppb
20.67
.5764
2.789
Mn2576
ppb
170.9
1.392
.3148
Ni2316
PPb'
12.18
.2914
2.593
PJ149
ppb
L28.32
10.4
36.71
Pb2203
ppb
186.0
2.226
1.196
Sb2063
ppb
8.237
2.066
25.08
Elems
Units
Avge
SOev
$RSD
Sel960
ppb
8.440
.5147
6.099
111908
ppb
L-1.782
.6325
35.5
Zn2062
ppb
1600.
22.71
1.419
224
-------
"Analysis (Sport Averages
Ned 10-08-97 00:59:04 AH page 17
Method: TRIANGL2 Sample Name: 183-3-18C Operator: DKH
Run Tine: 10/07/97 06:38 Filename: 100797
Mode: CONC Type: S Corr. Factor: 1.00000
Lab ID.: Cust. Smpl. ID.: Cust. ID.: 43231
Elems
Units
Avge
SDev
*RSD
C02286
ppb
L-6.784
1.356
19.99
AslSSO
ppb
L-5.449
3.78
69.37
Ba4934
ppb
3.570
.0803
2.249
Be3130
ppb
L.1541
.0252
16.36
Cd2265
ppb
40.73
1.03
2.528
Ag32SO
PPb
4.852
.1807
3.725
Eleins
Units
Avge
SOev
iRSD
Cr2677
PPb
18.91
4.946
26.16
Hn2576
ppb
12.07
.1103
.9141
N12316
ppb'
10.73
4.136
38.53
P.2149
ppb
69.81
16.94
24.27
Pb2203
ppb
189.2
.1989
.1051
Sb2063
ppb
5.944
5.273
88.7
Elems
Units
Avge
SDev
%RSD
Sel960
ppb
10.08
3.405
33.76
T11908
ppb
L-11.90
2.273
19.14
Zn2062
ppb
168.3
3.07
1.824
225
-------
•Analysis Report Averages
Ned 10-08-97 00:59:04 AM page 18
Method: TRIANGL2 Sample Name: 183-3-2C Operator: DKH
Run Time: 10/07/97 06:43 Filename: 100797
Mode: CONC Type: S Corr. Factor: 1.00000
Lab ID.: Cust. Sinpl. 10.: Cust. 10.: 43231
Eleins
Units
Avge
SDev
IRSD
Eleras
Units
Avge
SDev
*RSD
Hems
Units
Avge
SDev
%RSD
Co2286
ppb
L-4.216
.5978
14.18
Cr2677
ppb
18.73
1.465
7.822
Sel960
ppb
15.14
2.63
17.37
Asl890
ppb
L-2.845
1.803
63.37
Mn2576
ppb
9.917
.081
.8172
T11908
Ppb
L-9.613
3.033
31.56
Ba4934
ppb
3.441
.0877
2.548
N12316
ppb'
5.882
1.84
31.29
Zn2062
ppb
151.2
2.213
1.464
Be3130
PPb
L.1431
.0226
15.81
P.2149
ppb
110. 7
9.969
9.003
Cd2265
ppb
3.120
.3987
12.78
Pb2203
ppb
24.72
1.227
4.964
Ag3280
ppb
1.084
.291
26.83
Sb2068
ppb
5.600
3.057
54.59
-------
Rft'port Averages
Ned 10-08-97 00:59:04 AM page 19
Method: TRIANGL2 Sample Name: 183-3-2C PDS Operator: DKH
Run Time: 10/07/97 06:48 Filename: 100797
Mode: CONC Type: S Corr. Factor: 1.00000
Lab ID.: Cust. Smpl. ID.: Cust. ID.: 43231
Elems
Units
Avgs
SDev
IRSD
Elems
Units
Avge
SDev
%RSD
Elems
Units
Avge
SDev
*,RSD
C02286
ppb
45.78
.5609
1.225
Cr2677
ppb
65.84
1.093
1.66
Sel960
ppb
57.09
1.199
2.101
AS1890
ppb
42.67
1.859
4.357
Mn2576
ppb
59.62
.2415
.4051
T11908
ppb
44.99
2.69
5.979
8a4934
ppb
52.75
.1318
.25
Ni2316
ppb"
53.36
.3677
.689
Zn2062
ppb
343.1
3.282
.9565
Be3130
ppb
46.90
.3142
.6698
P_2149
ppb
108.0
4.079
3.776
Cd2265
ppb
52.22
.427
.8177
Pb2203
ppb
73.37
1.074
1.463
Ag3280
ppb
46.67
.2279
.4883
Sb2068
ppb
51.92
2.589
4.986
227
-------
.Analysis Report Averages Wed 10-08-97 00:59:04 AN page 20
Method: TRIAN6L2 Sample Name: 183-3-2C L Operator: DKH
Run Time: 10/07/97 06:52 Filename: 100797
Node: COHC Type: S Corr. Factor: 1.00000
Lab 10.: Cust. Sipl. ID.: Cust. ID.: 43231
Eleros
Units
Avge
SDev
*RSD
Co2286 As 18% 8a4934 Be3130 Cd2265 Ag3280
ppb ppb ppb ppb ppb ppb
L-1.161 L-.4891 L.6851 L.2191 L.4233 L.1553
.3492 .848 .0436 .0352 .0472 .4149
30.08 173.4 6.369 16.08 11.14 267.2
Eleras
Units
Avge
SDev
%RSD
Cr2677 Mn2576 Ni2316 P.2149 Pb2203 Sb2068
ppb ppb ppb- ppb ppb ppb
4.711 2.062 LI. 933 30.07 4.713 LI. 112
.4529 .022 .3797 4.359 1.025 .986
9.613 1.067 19.64 14.5 21.76 38.64
Elems 5el960 T11908 Zn2062
Units ppb ppb ppb
Avge 3.517 1.1127 32.23
SOev .9451 2.654 .2552
SRSD 26.37 2356 .7917
22S
-------
Analysis Report Averages
Wed 10-08-97 00:59:04 AH page 21
Method: TRIANGL2 Sample Name: 183-3-3C Operator: DKH
Run Tine: 10/07/97 06:57 Filename: 100797
lode: CONC Type: S Corr. Factor: 1.00000
Lab ID.: Cust. S«pl. 10.: Cust. ID.: 43231
Eleois
Units
Avge
SOev
*RSD
Eleois
Units
Avge
SOev
%RSD
Elens
Units
Avge
SOev
%RSD
Co2286
ppb
1-2.508
.8657
34.51
Cr2677
ppb
18.80
1.792
9.535
Sel960
PPb
6.414
.8551
13.33
AS1890
ppb
1-4.446
2.354
52.95
Mn2576
ppb
78.28
.4926
.6293
T11908
PPb
1-6.124
2.299
37.54
8a4934
ppb
15.26
.0256
.1676
NJ2316
ppb'
3.754
1.2
31.98
Zn2062
ppb
459.4
5.811
1.265
8e3130
ppb
L.1054
.0473
44.9
PJ149
ppb
121.7
4.906
4.03
Cd2265
ppb
1.109
.2281
20.56
Pb2203
ppb
95.22
1.243
1.305
Ag3280
ppb
1.419
.561
39.53
Sb2063
ppb
L2.873
3.743
130.3
-------
"•Analysis' Report Averages
Wed 10-08-97 00:59:04 AM page 22
Method: TRIANGL2 Sample Name: 183-3-3C DA Operator: DKH
Run Time: 10/07/97 07:02 Filename: 100797
Mode: CONC Type: S Corr. Factor: 1.00000
Lab ID.: Cust. Sipl. ID.: Cust. 10.: 43231
Elems
Units
Avge
SDev
*RSD
C02286 AS1890 8a4934 8e3130 Cd2265 Ag3280
ppb ppb ppb ppb ppb ppb
L-1.929 L-4.54S 15.18 L.0945 1.225 1.515
.5267 .4272 .0288 .0361 .3143 .4331
27.3 9.401 .1901 38.24 25.66 28.58
Elems
Units
Avge
SDev
%RSO
Cr2677
ppb
17.90
.847
4.733'
Mn2576
ppb
78.20
.272
.3478
Ni2316
ppb-
12.658
.695
26.14
P.2149
ppb
129.4
3.099
2.394
Pb2203
ppb
96.23
1.145
1.19
Sb2068
ppb
L3.852
.6
15.57
Elems
Units
Avge
SDev
SRSD
Sel960
PPb
5.137
.999
19.45
T11908
ppb
L-7.383
2.553
32.44
Zn2062
ppb
459.2
3.201
.6971
230
-------
'Analysis Report Averages
Wed 10-08-97 00:59:04 AM page 23
Method: TRIANGL2 Sample Name: 183-3-4C Operator: OKH
Run Time: 10/07/97 07:06 Filename: 100797
Mode: CONC Type: S Corr. Factor: 1.00000
Lab ID.: Cust. Snpl. ID.: Cust. ID.: 43231
[lens
Units
Avge
SDev
IRSD
Co2286 Asl890 Ba4934 8e3130 Cd2265 Ag3280
ppb ppb ppb ppb ppb ppb
L-2.251 L-2.307 7.222 L.2053 13.11 2.964
.5416 .263 .1023 .03 .169 .414
24.06 11.4 1.417 14.63 1.289 13.97
Elems
Units
Avge
SOev
*RSD
Cr2677 Mn2576 Hi2316 P.2149 Pb2203 Sb2068
ppb ppb ppb' ppb ppb ppb
13.07 640.4 LI. 556 131.1 483.0 4.079
.3783 3.483 .4508 8.039 6.131 3.553
6.72 .5439 28.97 6.131 1.269 87.1
El ens
Units
Avge
SOev
tRSD
Sel960
ppb
4.593
1.21
26.35
T11908
ppb
L-4.718
3.003
63.64
Zn2062
ppb
2404.
27.57
1.147
231
-------
Analysis Report Averages
10-08-97 00:59:04 AM page 24
Method: TRIANGL2 Sample Name: ICV/CCV Operator: DKH
Run Time: 10/07/97 07:12 Filename: 100797
Hode: CONC Type: 0 Corr. Factor: 1.00000
Lab 10.: Cust. Smpl. 10.: Cust. 10.: 43231
Eleios
Units
Avge
SDev
IRSO
[lens
Units
Avge
SOev
*RSD
Elens
Units
Avge
SOev
°<;RSD
Elects
Units
Avge
SOev
*RSO
Elems
Units
Avge
SDev
4RSO
Elems
Units
Avge
SDev
%RSD
Ag3280
ppb
498.0
2.278
.4574
Ca3179
Ppb
500.5
1.068
.2133
Fe2714
ppb
492.0
11.67
2.372
Na3302
ppffl
4.711
.1239
2.631
1960-1
ppb
488.5
1.767
.3613
H3349
ppb
495.1
1.004
.2027
A13082
ppb
522.4
10.14
1.942
Cd2265
ppb
499.5
1.732
.3467
K_7664
ppro
4.736
.0482
1.018
Ni2316
opb
498.4
1.254
.2516
1960-2
ppb
494.2
2.397
.5861
T11908
ppb
503.5
1.788
.3552
Asl390
ppb
499.4
1.46
.2923
Ce41S6
ppb"
493.0
3.176
.6443
Li6707
ppb
464.2
5.36
1.155
P.2149
ppb
501.6
3.926
.7827
Pb2203
ppb
496.2
2.997
.6035
V.2924
ppb
496.5
.9821
.1978
B.2496
ppb
3099.
361.8
11.67
C02286
ppb
493.8
1.317
.2667
Hg2790
ppb
497.2
2.444
.4915
2203-1
Ppb
488.5
1.726
.3534
Sel960
ppb
492.3
2.519
.5115
Zn2062
ppb
496.6
3.39
.6826
Ba4934
ppb
489.6
.6792
.1387
Cr2677
ppb
500.1
1.846
.369
Mn2576
ppb
496.0
1.26?
.2553
2203-2
ppb
500.1
4.653
.93U
Snl899
ODD
Q9392.
48.24
.5136
Si2881
ppb
017090.
245.4
1.424
Be3130
ppb
490.7
2.24
.4565
Cu3247
ppb
492.5
3.788
.769
Mo2020
ppb
493.6
1.95
.3952
Sb2068
bob
488.?
1.181
.2416
Sr42l5
ppb
491.5
.1941
.0395
232
-------
'•Analysis Report ftverages
Wed 10-08-97 00:59:04 AN page 25
Method: TRIANGL2 Sauple Name: IC8/CCB Operator: DKH
Run Time: 10/07/97 07:17 Filename: 100797
Mode: CONC Type: Q Corr. Factor: 1.00000
Lab 10.: Cust. Sipl. 10.: Cust. 10.: 43231
Eleras
Units
Avge
SDev
%RSO
Eleras
Units
Avge
SDev
IRSD
Elems
Units
Avge
SDev
*RSD
Elens
Units
Avge
SDev
4RSD
cleus
Units
Avgs
SDev
*RSD
tieros
Units
Avge
SDev
%RSD
Ag3280
ppb
.5632
.4598
81.64
Ca3179
ppb
-2.486
.4173
16.79
Fe2714
ppb
.8134 .
4.334
532.8
Na3302
ppm
.0185
.0943
510.3
1960-1
ppb
4.275
.3584
20.08
Ti3349
ppb
.4956
.1189
24
A13082
ppb
36.66
4.451
12.14
Cd2265
ppb
.2293
.2363
103.1
KJ664
ppiB
.0607
.0181
29.75
Ni2316
ppD
.9271
.4753
51.27
1960-2
opb
-.4360
1.606
363.4
T11903
ppb
Q7.715
4.843
62.78
AS 1890
PPb
1.069
1
93.54
Ce4186
ppb-
-.0852
.527
618.3
Li6707
PPb
.5874
.1166
19.85
P.2149
PPb
6.954
3.465
49.83
Pb2203
ppb
-.5180
.9348
130.5
V.2924
opb
1.815
.1197
6.593
B.2496
ppb
2589.
228.7
8.835
Co2236
ppb
.1817
.0916
50.41
Mg2790
ppb
1.017
1.452
142.3
2203-1
ppb
1.120
3.329
297.3
Sel960
ppD
1.133
.91
30.34
2n2062
opo
.7824
.0212
2.713
Ba4934
ppb
.42^8
.1381
32.13
Cr2677
PPb
1.091
.03^7
3.641
Mn25-6
ppb
.5471
.146
26.69
2203-2
ppo
-1 .336
1.426
106.3
Snl399
ppb
Q1S.73
7.422
39. o2
Si286l
opb
012830.
730.1
5.692
6e3130
ppb
.7008
.1876
26.77
Cu3247
PPb
-.9285
.3665
39.47
flo2020
ppb
1.502
.4715
31.39
5b2C63
ppb
3.275
1.41
43.06
Sf4215
opb
.4860
.1582
32 . 55
233
-------
'Analysis' Report Averages
Wed 10-08-97 00:59:04 AM page 26
Method: TRIANGL2 Sample Name: 183-3-5BC Operator: DKH
Run Time: 10/07/97 07:23 Filenaue: 100797
Mode: CONC Type: S Corr. Factor: 1.00000
Lab ID.: Oust. Sipl. ID.: Cust. ID.: 43231
Elens
Units
Avge
SDev
$RSD
Elents
Units
Avge
SDev
$RSD
Eleios
Units
Avge
SDev
SRSD
Co2286
ppb
L-1.457
.4882
33.51
Cr2677 Hn2576
ppb ppb
5.442 9.5CT4
.5392
9.908 /.3263
JK2316
/ppb-
T11908 Zn2062
ppb ppb
12.77 1-2.601 114.6
.7102 .5646 .9378
Cd2265 Ag3280
ppb ppb
1.687. L.8616
.2192 .5426
13 62.97
Sb2068
ppb
LI.901
1.328
69.85
Se
234
-------
1 Analysis Report Averages
Wed 10-08-97 00:59:04 AM page 27
Method: TRIANGL2 Sample Name: 183-3-6C Operator: DXH
Run Time: 10/07/97 07:27 Filename: 100797
Mode: CONC Type: S Corr. Factor: 1.00000
Lab ID.: Cust. Sipl. ID.: Cust. ID.: 43231
El ems
Units
Avge
SDev
%RSD
Co2286
Ppb
L-1.526
.4706
30.84
As 1890 "
ppb
L-3.844
.889
23.12
~Ba4934
ppb
3.043
.0476
1.566
Be3130
ppb
L.2005
.045
22.45X
Cd2265
PPb >
L.8JJ&S
.x-f395
15.7
AjjSttO
xtfpb
L.8136
.4068
50
El eras
Units
Avge
SDev
%RSD
Cr2677
ppb
8.543
.4332
5.071
«n2576
ppb
7.011
.0662 /
.9436/
Ni2316>
PPb/
1/3612
/:5791
160.3
"PJ2149
ppb
91.00
1.274
1.401
Pb2203
ppb
15.54
.8226
5.294
Sb2068
PPb
LI. 250
1.429
114.3
El eras
Units
Avgs
SDev
%RSD
Sel960
PPb
3.292
1.635
49.65
ppb
[L-2.546
^^JAT" —
17.56
Zn2062
PPb
235
-------
Analysis Report Averages
Wed 10-08-97 00:59:04 AH page 28
Method: TRIANGL2 Sample Name: 183-5-7C Operator: DKH
Run Time: 10/07/97 07:32 Filenane: 100797
Node: CONC Type: S Corr. Factor: 1.00000
Lab 10.: Cust. Sipl. 10.: Cust. 10.: 43231
Elens
Units
Avge
SDev
IRSD
Co2286
PPb _
L-1.108
.506
45.66
AS1890
_ppb •
1-3.723
1.631
43.82
Ba4934
^*r~~*"
-PPD
7.064
.061
.8632
J&&KT
ppb
L.1714
.0323
18.85
•"U32265
ppb
L.783?
.318^*
40xSf
AQ3280
ppb >
M70
<4752
40.62
Eleins
Units
Avge
SOev
%RSD
Cr2677
ppb
10.57
.6398 '
6.054
Mn2576
PPb
8.516
.1143
1.342 >
N12316
ppb'
l.SMK
J&l
M21.2
P 2JW1
/p|b
113.3
3.448
3.044
Pb2203
ppb
21.08
.7887
3.74
Sb2068
ppb
L3.022
3.133
103.7
-\
Elems
Units
Avge
SDev
Sel960 U1908
ppb /ppb
14.3 L-4.576
.6368
475 13.92
23B
-------
'Analysis Report Averages
Ned 10-08-97 00:59:04 AM page 29
Method: TRIANGL2 Sample Name: 183-3-8C Operator: DKH
Run Time: 10/07/97 07:38 Filename: 100797
Mode: CONC Type: S Corr. Factor: 1.00000
Lab ID.: Cust. Srapl. ID.: Cust. ID.: 43231
[leas
Units
Avge
SDev
*RSD
Eleras
Units
Avge
SDev
*RSD
Elems
Units
Avge
SDev
°.RSD
C02286
PPb
L-1.817
^Ivvv
38.89
Cr2677
PPb
9.054
.5541
6.12
Sel960
PPb/
3/20
/96
5.27
AS1890
ppb
1.642
40.76
Mn2576
PPb
16.10
.1184
.735/
/11908
ppb
L-6.378
.3194
5.008
Ba4934
Pfib — *"
3.645
.084
2.304
Ni2316
PPb' /'
7,4i6
X7708
10.39
Zn2062
ppb
140.1
2.001
1.428
8e313j).
•"ppb
L.1906
.039
20.47
R^-2149
Xppb
110.3
1.194
1.083
Pb2203
ppb
23.83
1.196
5.021
T7658
.5403
70.56
Sb2068
ppb
LI.887
1.519
80.52
231
-------
Analysis'Report Averages
Wed 10-08-97 00:59:04 AH page 30
Method: TRIANGL2 Sample Name: 43231 MB
Run Time: 10/07/97 07:42 Filename: 100797
Mode: CONC Type: S Corr. Factor:
Lab ID.: Oust. Sopl. ID.
Eleis Co2286 Asl890
Units ppb ppb
Avge L-.7094 L-1.691
SDev .2122 .7641
*RSO 29.92 45.2
Operator: DKH
1.00000
43231
0078
3.756
Ag3280
ppb ppb
L-.3305 L.2580
.3004 .0152
90.9 5.899
Pb2203
ppb
2.021
.8474
41.94
238
-------
'Analysis Report Averages
Wed 10-08-97 00:59:04 AN page 31
Hethod: TRIAN6L2 Sample Name: 43231 LCS Operator: DKH
Run Time: 10/07/97 07:47 Filename: 100797
Node: CONC Type: S Corr. Factor: 1.00000
Lab ID.: Cust. Sapl. ID.: Cust. ID.: 43231
El ems
Units
Avge
SDev
IRSD
C02286 AS1890 8a4934 Be3130 Cd2265 Ag3280
ppb ppb ppb ppb ppb ppb/"
46,18 44.02 46.31 44.62 46.76 /43.15
.5436 .6175 .0547 .1791 .08^X^.223
1.177 1.403 .1181 .4014 ^Hll .5168
r\
El eras
Units
Avge
SOev
IRSO
Cr2677
ppb
47.61
.4845
1.018
Nn2576
PPb
47.38
.1828
.38S8/
Ni2316
PPb' /
4#fo
X2643
.5886
B/Z149
'PPb
903.1
5.482
.6071
Pb2203
ppb
45.36
.5191
1.132
Sb2068
ppb
46.84
1.144
2.442
Elems
Units
Avge
SDev
*RSD
Sel960 /T11908
ppb / ppb
89 49.42
509 2.208
.017
Zn2062
PPb
189.3
1.914^
.011
239
-------
Analysis Report Averages
Bed 10-08-97 00:59:04 Ad page 32
Hathod: TRIANGL2 Sample Name: 184-23-1A8 Operator: DKH
Run Tine: 10/07/97 07:52 Filenaue: 100797
Node: CONC Type: S Corr. Factor: 1.00000
Lab 10.: Cost. Sipl. 10.: Cust. ID.: 43231
Elens
Units
Avge
SDev
%RSD
El ems
Units
Avge
SDev
*RSD
Elens
Units
Avge
SDev
*RSO
Co2236
ppb
220.5
3.464
1.571
Asf
ppb
1146.
7.119
.6212
Cr2677 Hn2576
ppb ppb
9376. H119800.,
26.18 1600
.2792 1
/
Sel960/T11908
ppb / ppb
».9 365.8
PPb
12090.
23.41
.1937
Ni2316
'1975.
.7151
.0362
SS3T30
ppb
7.474
.5287 >
7. OK
s
PJ149
ppb
14070.
18.81
.1337
Cd2265
PPb /
2ȣ
^.54
.1549
Pb2203
ppb
H515300.
3877
.7524
Ag«280
ppb
104.3
2.228
2.136
Sb2068
PPb
6628.
16.15
.2437
240
-------
Analysis Report Averages
Wed 10-08-97 00:59:04 AH page 33
Method: TRIAN6L2 Sample Name: ICB/CCB Operator: DXH
Run Time: 10/07/97 10:36 Filename: 100797
Mode: COHC Type: 0 Corr. Factor: 1.00000
Lab ID.: Cust. Sipl. 10.: Cust. ID.: 43231
Elems
Units
Avge
SOev
*RSD
Elems
Units
Avge
SOev
%RSD
El eras
Units
Avge
SOev
*RSO
Ag3280 A13082
ppb ppb"
-.0062 059.41
.1122 1.81
1811 3.047
Ca3179 Cd2265
ppb ppb
-3.314 -.0176
,266 .1117
8.028 633.6
Asl890 8.2496
8a4934
tfr
27.91
CU3247
ppb ppb
.1885 -.2727
.1585 .1278
34.08 46.85
Fe2714
ppb
-3.106
9.028 yo02
K 7664 ,116707
~ / .
ppra /• ppb
.1566
.0024
290.6.' 4.07
1.547
NJ2316
ppb
.0409 2.079
.0453 .3544
110.9 17.05
?b2203
ppb
0-2.166
Hg2790 Mn2576 Mo2020
ppb ppb ppb
-.1193 -.0542 -.6430
1.226 .0354 .0585
1028 65.4 9.0jr~
575.5
SnlS99 S.-4215
ppb ppb
Q81.00 .0037
.0125
9.497^ IT?
Elems
Units
Avge
SDev
*RSD
H3349 T11908
ppb ppb
-.0439 4.802
.1148 .1333
261.4 2.775
V.2924
ppb
.4958
.0568
11.46
Zn2062
PPb
7.076
.225
3.18
Si2881
PPb
Q-57S.7
2.038
.354
241
-------
Analysis. Report Averages
Wed 10-08-97 00:59:04 AH page 34
Method: TRIAN6L2 Sample Name: ICV/CCV Operator: DKH
'Run Tine: 10/08/97 00:37 Filename: 100797
Node: CONC Type: Q Corr. Factor: 1.00000
Lab ID.: Cust. Smpl. ID.: Cust. ID.: 43231
Elems
Units
Avge
SDev
*RSD
Eleins
Units
Avge
SOev
IRSD
Eleias
Units
Avge
SDev
*RSD
El eras
Units
Avge
SDev
SRSD
Elems
Units
Avge
SDev
*RSD
Eleras
Units
Avge
SDev
SRSD
Ag3280
ppb
487.2
2.254
.4628
Ca3179
ppb
505.1
3.893
.7706
Fe2714
ppb
494.4
15.34
3.103
Na3302
ppiB
Q4.108
.0994
2.42
1960-1
ppb
445.1
1.342
.3016
Ti3349
ppb
515.2
1.203
.2334
A13082
ppb
0669.4
11.67
1.743
Cd2265
ppb
504.7
2.822
.5592
KJ664
ppm
Q4.393
.0173
.4043
(U2316
ppb
498.1
2.722
.5465
1960-2
ppb
480.7
4.53
.9423
T 11903
ppb
499.0
11.63
2.332
Asl890
ppb
487.8
1.722
.353
Ce4186
ppb"
498.5
1.957
.3925
Li6707
ppb
9448.3
3.613
.3058
P.2149
opt)
477.5
3.S26
.8013
Pb2203
ppb
500.7
3.405
.6801
V_2924
ppb
485.3
1.753
.3609
B_2496
ppb
281.0
2.616
.9308
Co2286
ppb
481.9
2.348
.591
Plg2790
pDD
495.6
5.718
1.154
2203-1
ppo
480.1
2.576
.5366
Sel960
ppb
468.9
2.6
.5545
Zn2062
ppb
472.4
4.312
1.019
8a4934
ppb
501,?
1.313
.2616
Cr2677
ppb
502.3
3.181
.6333
Hn257c
ppb
497.0
2.233
.-5502
2205-2
ppo
511.1
5.641
1.104
Snl899
ppb
Q9309.
68.76
.7387
Si2881
ppb
Q-467 .6
1.7
.3635
Be3130
ppb
457.8
2.689
.5873
Cu3247
PPb
493.8
3.596
.721
1102020
ppb
495.6
2.781
.5654
3b2068
ppo
487.4
2.899
.5949
Sr4215
ppb
516.2
1.045
.2024
242
-------
ftnjlysis Report Averages
Hed 10-08-97 00:59:04 AH page 35
Method: TRIAN6L2 Sample Name: ICB/CC8 Operator: DKH
jn Tine: 10/08/97 00:42 Filename: 100797
Jde: CONC Type: Q Corr. Factor: 1.00000
Lab ID.: Cust. Smpl. ID.: Cust. ID.: 43231
tlems
Units
/ge
-Dev
*RSD
leras
Units
*vge
Dev
«RSO
lens
.nits
Avge
Dev
RSO
-'leas
nits
Hvge
SDev
:RSO
El ems
nits
vge
SDev
"-RSO
clems
Units
vge
.Dev
*RSD
Ag3280
ppb
.3916
.2666
68.08
Ca3179
ppb
-7.189
.6779
9.43
Fe2714
ppb
5.411
2.229
41.2
Na3302
ppm
-.0370
.0605
163.3
1960-1
ppb
-6.508
.8738
13.43
Ti3349
ppb
.4906
.0553
11.26
A13082
ppb
Q182.6
7.268
3.979
Cd2265
ppb
.3826
.1892
49.45
K_7664
ppm
-.0233
.0145
62.28
Ni2316
ppD
-.1446
.6003
415.3
1960-2
ppb
3.181
1.012
31.33
111908
ppb
Q9.320
4.261
45.72
AS1890
ppb
-1.629
2.214
136
C64186
ppb-
.2814
.8087
287.4'
Li6707
ppb
.5986
.0413
6.903
P.2149
pob
-5.639
1.584
28.08
?b2203
ppb
.6493
.3022
46.55
V.2924
ppb
Q4.559
.4512
9.897
8.2496
ppb
-221.3
.3662
.1655
C02286
ppb
-.0945
.1859
196.8
Mg2790
ppb
1.866
.6428
34.45
2203-1
ppb
4.249
1.159
27.29
Sel960
ppb
-.0454
.4245
934
Zh2Q62
ppb
1.345
.2023
15.04
Ba4934
ppb
.4201
.0557
13.27
Cr2677
ppb
.5804
.3297
56.8
Mn2576
ppb
.5211
.0456
8.742
2203-2
ODD
-1.1*3
1.027
89.52
Snl89
opb
Q-27.57
34.92
126.7
Si288i
ppb
0-768.3
1.751
.228
8e3130
ppb
Q2.340
.0934
3.289
Cu3247
ppb
Q-3.335
.0785
2.354
1102020
ppb
1.531
.5562
36.47
Sb2068
ppb
3.183
2.248
7C.64
Sr4215
PPb
.4776
.035
7.337
243
-------
(*?)aly,slstReport Averages
Wed 10-08-97 00:59:04 AH page 36
Method: TRIANGL2 Sample Name: ICSA8 Operator: DKH
Run Time: 10/08/97 00:47 Filename: 100797
Mode: CONC Type: Q Corr. Factor: 1.00000
Lab ID.: Cust. Sropl. 10.: Cust. ID.: 43231
El eras
Units
Avge
SDev
%RSD
Elems
Units
Avge
SDev
*RSD
Elens
Units
Avge
SDev
*RSD
Elens
Units
Avge
SOev
USD
Elems
Units
Avge
SDev
SREO
Elens
Units
Avge
SDev
*RSD
Ag32SO
ppb
528.1
1.92
.3636
Ca3179
ppb
462200.
944.6
.2044
Fe2714
ppb
175500.
208.4
.1188
Na3302
ppiB
4.689
.066
1.407
1960-1
pob
495.8
5.425
1.094
Ti3349
PPb
516.2
.5002
.0969
A13082
ppb
497300.
3913
.7868
Cd2265
ppb
482.4
.8757
.1815
K_7664
ppi»
Q23.40
.0206
.088
Ni2316
ppb
461.5
1.79
.3879
1960-2
ppb
509.0
4.32
.947
T11908
PPB
516.0
16.55
3.207
ASJS90
ppb
515.6
2.538
.4922
Ce4186
ppb-
505.6
1.849
.3658
Li6707
ppb
588.0
1.016
.1728
P_2149
ppb
499.3
7.667
1* * f
.300
Pb2203
PPb
491.3
2.908
.5919
V_2924
ppb
485.0
1.39
.2866
BJ496
ppb
313.4
.6637
.2118
C02286
ppb
461.2
.978
.2121
Hg2790
ppb
527200.
761.9
.1445
2203-L
PPb
498.8
5.345
1.072
Sel960
ppb
504.6
1.604
.3173
Zn2062
ppb
428.6
3.987
.9303
8a4934
ppb
524,2
1.87
.3568
Cr2677
ppb
486.7
1.406
.2888
Mn2576
ppb
463.7
1.351
.2913
2203-2
oob
'487.6
6.914
1.418
Snl899
ppb
Q9775.
54.97
.5624
Si2381
ppb
Q-172.7
4.416
2.557
Be3130
ppb
458.3
1.521
.3319
Cu3247
ppb
540.7
3.726
.6891
M02020
ppb
493.2
2.742
.5504
Sb2068
ppb
510.8
4.903
.9609
SN215
ppb
531.1
1.389
.2615
244
-------
AutoSapf'er Report Table: HA452
Red 10-08-97 02:10:19 AH page 1
fable Name: HA452 Autosanpler Type: TYPE TJA
. Sample Positions: 170/192 QC Positions: 13/19 It Sets: 1
Rinse Station location is rack -1, DOS. -1.
*Pos Left Analyses/Pos
— Racks —
'Hack ft Type
1
2
3
4
5
Aux. (I) Rack
Sample (16nn)
Sample (16mm)
Sample (16m)
Sample (16mm)
Usage
STD/OC/8LANK
Samples
Samples
Samples
Samples
13
,26
48
48
48
10
1
1
1
1
— Sample Sets —
Sett Type Prepare? Description
1 Normal No 43231
— Preparation Info —
Sett Uptake Uptake«2 Final
Method «Pos Rack! StartPos
TRIAN6L2 22 2 1
Oil.Factor
No Samples Prepared.
Rack HI
Pos Row Col Sample Name
Set It aused
Type
1
2
3
4
5
6
(7..
1
1
1
1
1
1
.19
1
2
3
4
5
6
Not
STD3
STD1-BLANK
ICSA8
CHECK LO
ICV/CCV
ICB/CCB
Used)
-NA-
-NA-
-NA-
-NA-
-NA-
-HA-
2
1
2
1
4
4
Standard 1'
Standard
OC Standard
QC Standard
QC Standard
QC Standard
-c,\- \
Rack 112
Pos Row Col Sample Naae
Set i «Used Type
I
2
3
4
5
6
7
8
9
10
11
12
13
14
IS
I
1
1
1
I
1
1
1
1
1
1
1
2
2
2
1
2
3
4
5
6
7
8
9
10
11
12
1
2
3
183-3-38 X50
183-3-38 X50 DA ]
183-3-58C
183-3-6C
183-3-7C
183-3-8C
43231 MB
43231 LCS
184-23-1A8
184-23-2A8
184-23-2AB
184-23-3A8
184-23-3AB
184-23-4A8
184-23-6AB
1
1
]
xso
XSO ]
XSO L
XSO
XSO DA
XSO
XSO
I -NA- Sample
-NA- Sample
1 -NA- Sample
-NA- Sample
1 -NA- Sample
-NA- Sample
[ -NA- Sample
-NA- Sampl.e
-NA- Sample
-NA- Sample
-NA- Sample
-NA- Sample
-NA- Sample
-NA- Sample
-NA- Sample
245
-------
.,AutoSat»pler Report Table: HA452 Hed 10-08-97 02:10:19 AN page 2
«> >
Rack 12
*
Pos Row Col Sample Name Set 8 (Used Type
16
17
18
19
20
21
22
(23.
2
2
2
2
2
2
2
..48
4 184-23-7AB XSO
5 184-23-8A8 XSO
6 184-23-9AB XSO
7 184-23-10AB.5 XSO
8 183-15-1C
9 laS-lS-lBj?1*^,,^.,,^,^
10 ( empty )
Not Used)
I
1
1
1
1
t 1
1
-NA-
-NA-
-NA-
-NA-
-NA-
-NA-...
-NA-
Saaple
Sample
Sample
Sample
Sample
Saaple
-NA-
Rack 83
Pos RON Col Sample Name Set 8 lUsed Type
(1...48 Hot Used)
Rack «4
Pos RON Col Sample Name Set 8 8Used Type
(1...48 Not Used)
Rack 85
Pos RON Col Sample Name Set i ttUsed Type
(1...48 Not Used)
246
-------
Analysis Report Averages
Hed 10-08-97 07:03:45 AN page 4
Method: TRIANGL2 Sample Name: STD1-BLANK Operator:
Run Tine: 10/08/97 02:11 Filenane: 100797
Mode: IR Type: X Corr. Factor: 1.00000
Lab ID.: Oust. Snpl. ID.: Cust. ID.:
Elens Ag3280 A13082 As1890 B.2496 Ba4934 8e3130
Units count count count count count count
Avge 0 .00575 -.0004 .0037 .00062 .00085
SDev .00011 .00009 .00006 .00018 .00001 .00002
tRSO 18087.5 1.71474 15.4235 5.05971 1.86892 2.9699
Eleus Ca3179 Cd2265 Ce4186 Co2286 Cr2677 Cu3247
Units count count count count count count
Avge .00033 -.00009 -.00005 -.00016 -.0001 .00229
SDev .00001 .00019 .00009 .00003 .00005 .00004
*RSD 5.19045 209.65 184.618 22.4583 50.3011 1.84165
Elems Fe2714 K.7664 Li6707 Mg2790 Hn2576 Ho2020
Units count count count count count count
Avge .00005 3.89015 .07635 .00013 .00003 .00006
SDev .00003 .02683 .00034 .0001 0 .00004
*RSD 57.6222 .6897 .44804 77.3615 11.5067 74.4291
Eleus Na3302 Ni2316 P.2149 2203-1 2203-2 Sb2068
Units count count count count count count
Avge .00104 -.00168 -.00093 .00173 .00004 .00073
SDev .00226 .00018 .00003 .00048 .00016 .00022
*RSD 216.865 10.7239 3.77577 28.1234 384.12 30.9777
Eleras 1960-1 1960-2 Snl899 Sr4215 Ti3349 T11908
Units count count count count count count
Avge -.00648 .00232 -.0004 .00033 .00016 -.00034
SDev .00038 .00034 .00013 .00001 .00011 .00007
*RSO 5.86225 14.9219 33.245 5.3312 72.6622 22.7504
Elems V_2924 Zn2062 Si2881
Units count count count
Avge -.00032 .00008 .01863
SOev .00002 .00003 .00002
*RSD 7.08465 42.1786 .15691
247
-------
( Analysis Report Averages
Ned 10-08-97 07:03:45 AH page 5
Method: TRIAN6L2 Sample Name: STD3 Operator:
Run Tiie: 10/08/97 02:16 Filename: 100797
Hode: IR . Type: X Corr. Factor: 1.00000
Lab ID.: Oust. Sopl. ID.: Cust. ID.:
Elens Ag3280 A13082 Asl890 8.2496 Ba4934 Be3130
Units count count count count count count
Avge .38497 .02043 .05097 .16505 .2893.7 .23431
SOev .0015 .00034 .00013 .00019 .00036 .00102
tRSD .39163 1.67379 .26263 .11973 .12707 .43841
Elens Ca3179 Cd2265 Ce4186 Co2286 Cr2677 Cu3247
Units count count count count count count
Avge .02224 .92028 .11079 .10035 .14505 .17642
SDev .00008 .00407 .00011 .00035 .00044 .00115
IRSD .36079 .44328 .10096 .34883 .30798 .65246
Elens Fe2714 KJ664 Li6707 Hg2790 Mn2576 Mo2020
Units count count count count count count
Avge .00408 21.8268 14.981 .01976 .12633 .07576
SDev .00002 .02927 .03249 .00001 .00044 .0004
IRSD .72347 .13412 .2169 .08686 .35048 .53452
Eleis Na3302 Ni2316 PJ149 2203-1 2203-2 Sb2068
Units count count count count count count
Avge .19977 .3416 .02126 .16974 .08997 .11321
SDev .00347 .00095 .0002 .00103 .00037 .00035
*RSD 1.74049 .27985 .96336 .6079 .4169 .31007
Elesis 1960-1 1960-2 Snl899 Sr4215 H3349 T11908
Units count count count count count count
Avge .24882 .15605 .10968 .83545 1.11886 .03102
SDev .00183 .00038 .00038 .00054 .00186 .00081
*RSD .73765 .24925 .35463 .06528 .16681 2.62214
Elens VJ924 Zn2062 Si2881 Pb2203 Sel960
Units count count count
Avge .03661 .09328 .46311
SDev .00009 .00065 .0027
*RSD .24992 .69981 .58429
248
-------
Analysis Report Averages
Wed 10-08-97 07:03:45 AH page 6
Method: TRIANGL2 Saaple Name: STD3 Operator: DKH
Run Tiae: 10/08/97 02:21 Filename: 100797
Node: CONC Type: 0 Corr. Factor: 1.00000
Lab ID.: Cust. Sipl. ID.: Cust. ID.: 43231
[leas
Units
Avge
SOev
tRSD
Eleins
Units
Avge
SOev
tRSD
Elens
Units
Avge
SDev
IRSO
Elems
Units
Avge
SDev
tRSD
Elens
Units
Avge
SDev
tRSD
Elens
Units
Avge
SDev
tRSD
Ag3280
PPb
999.7
3.694
.3695
Ca3179
ppb
1003.
4.529
.4516
Fe2714
PPb
997.5
• 10.97
1.1
Ha3302
ppffl
9.832
.1523
1.549
1960-1
ppb
1006.
3.246
.3227
V.2924
PPb
1003.
3.042
.3034
A13082
ppb
993.9
22.08
2.221
Cd2265
ppb
1003.
3.344
.3335
KJ664
PP»
9.993
.0422
.4221
Ni2316
ppb
1003.
2.648
.264
1960-2
ppb
1006.
3.149
.313
Zn2062
ppb
1007.
7.998
.7942
Asl890
ppb
1000.
1.654
.1653
Ce4186
ppb"
1003.
1.126
.1123
Li6707
ppb
998.7
5.033
.5039
P.2149
ppb
1009.
9.913
.9826
Snl899
PPb
1003.
2.994
.2985
S12881
ppb
10010.
56.74
.5668
8.2496
ppb
1002.
2.889
.2885
Co2286
ppb
1006.
4.499
.4474
Mg2790
PPb
1001.
2.48
.2478
2203-1
PPb
1004.
1.374
.1369
Sr4215
ppb
999.2
.7262
.0727
Pb2203
ppb
1001.
5.384
.5381
Ba4934
PPb
1002.
1.711
.1708
Cr2677
PPb
1003.
4.471
.4459
Hn2576
PPb
1003.
3.55
.3541
2203-2
PPb
999.0
8.544
.8553
Ti3349
PPb
1001.
1.892
.1891
Sel960
PPb
1006.
1.368
.136
Be3130
ppb
1003.
5.617
.5601
Cu3247
ppb
999.9
6.198
.6199
M02020
ppb
1007.
3.101
.308
Sb2068
ppb
1010.
3.96
.3922
T11908
ppb
1022.
9.04
.8842
249
-------
t Analysis Report Averages
Ned 10-08-97 07:03:45 AH
page
Method: TRIANGL2 Sample Name: ICV/CCV Operator: 0KB
Run Tine: 10/08/97 02:30 Filename: 100797
node: CONC Type: Q Core. Factor: 1,00000
Lab ID.: Cust. Snpl. ID.: . Cust. ID.: 43231
Eleins
Units
Avge
SDev
USD
Eleas
Units
Avge
SDev
*RSD
Elens
Units
Avge
SDev
IRSD
Elens
Units
Avge
SDev
IRSD
Elens
Units
Avge
SDev
IRSO
El ems
Units
Avge
SDev
«SD
Ag3280
ppb
506.6
2.069
.4084
Ca3179
ppb
509.4
1.249
.2451
Fe2714
PPb
499.8
5.532
1.107
Na3302
PPa
4.978
.0322
.6475
1960-1
PPb
513.1
1.586
.3091
Ti3349
ppb
503.1
.819
.1628
A13082
ppb
486.5
14.52
2.985
Cd2265
ppb
506.5
1.425
.2814
K.7664
ppm
4.906
.0102
.2079
Ni2316
ppb
504.9
1.326
.2626
1960-2
ppb
513.0
2.484
.4843
T11908
ppb
509.9
9.537
1.87
AS1890
ppb
510.4
3.431
.6722
Ce4186
ppb-
501.5
2.827
.5637
Li6707
PPb
487.2
2.955
.6065
P.2149
ppb
510.7
2.84
.5561
Pb2203
PPb
505.3
.7743
.1532
V.2924
ppb
506.1
1.137
.2245
8,2496
ppb
500.3
.4603
.092
Co2286
ppb
506.8
1.968
.3884
Mg2790
ppb
504.8
1.273
.2521
2203-1
ppb
505.2
2.572
.509
Sel960
PPb
513.0
2.144
.4179
Zn2062
PPb
508.5
3.839
.7549
834934
ppb
503,2
1.02
.2027
Cr2677
ppb
504.7
2.504
.4961
«n2576
ppb
504.7
1.411
.2796
2203-2
ppb
505.4
2.418
.4785
Snl899
ppb
506.3
1.696
.3349
S12831
ppb
0285.1
1.762
.6179
8e3130
ppb
506.9
2.192
.4324
CU3247
ppb
505.9
3.263
.6449
H02020
PPb
505.8
1.662
.3286
Sb2068
PPb
525.7
3.273
.6226
Sr4215
ppb
502.4
.6403
.1274
250
-------
Analysis Report Averages
Ned 10-08-97 07:03:45 AN page 9
Method: TRIANGL2 Sample Nane: ICB/CCB Operator: DKH
Run Tine: 10/08/97 02:36 Filenaie: 100797
Hode: CONC Type: Q Corr. Factor: 1.00000
Lab ID.: Cust. Sipl. ID.: Cust. ID.: 43231
Elens
Units
Avge
SOev
USD
Elens
Units
Avge
SOev
%RSD
Eleis
Units
Avge
SDev
*RSD
Elens
Units
Avge
SDev
tRSD
Elens
Units
Avge
SDev
tRSD
Elens
Units
Avge
SDev
tRSD
Ag3280
ppb
.5272
.5009
95
Ca3179
ppb
1.373
.426
31.03
Fe2714
ppb
-2.411
9.886
410.1
Na3302
ppra
.0391
.1478
377.6
1960-1
ppb
1.869
1.721
92.09
H3349
ppb
.4260
.0588
13.79
A13082
ppb
-19.13
8.006
41.86
Cd2265
ppb
.4632
.1585
34.23
K.7664
PPn
.0333
.0201
60.48
1)12316
ppb
.8217
.5218
63.5
1960-2
PPb
-3.037
.3126
10.29
T11908
PPb
2.965
3.467
116.9
AS1890
ppb
1.761
.2552
14.49
Ce4186
ppb'
1.727
.8644
50.06
116707
ppb
.4562
.0671
14.72
P.2149
ppb
2.982
1.86
62.36
Pb2203
ppb
-1.007
.8433
83.75
V.2924
ppb
.4220
.1185
28.08
8.2496
ppb
.0299
.4995
1673
C02286
ppb
.6189
.1793
28.97
Mg2790
ppb
-1.801
2.625
145.7
2203-1
ppb
-3.283
2.134
65
Sel960
ppb
-1.403
.478
34.07
Zn2062
ppb
-.5546
.1114
20.09
8a4934
ppb
.3951
.1296
32.8
Cr2677
ppb
.4277
.3855
90.14
Mn2576
ppb
.3929
.0796
20.27
2203-2
ppb
.1296
2.242
1730
Snl899
ppb
.5508
.7697
139.8
S12881
ppb
.8372
1.813
216.6
8e3130
ppb
.1292
.1933
149.5
CU3247
ppb
.3246
.3636
112
1102020
ppb
.8313
.227
27.3
Sb2068
ppb
.8309
1.405
169.1
Sr4215
ppb
.4123
.1
24.25
251
-------
. Analysis Report Averages
Wed 10-08-97 07:03:45 AH page 10
Method: TRIANGL2 Sample Name: ICSA8 Operator: DKH
Run Tine: 10/08/97 02:41 Filenane: 100797
Node: CONC Type: 0 Corr. Factor: 1.00000
Lab ID.: Cust. S»pl. ID.: Cust. ID.: 43231
Eleos
Units
Avge
SDev
IRSD
Eleas
Units
Avge
SDev
IRSO
Eleos
Units
Avge
SDev
%RSD
Eleins
Units
Avge
SOev
%RSD
Eleos
Units
Avge
SDev
IRSD
Elens
Units
Avge
SDev
IRSD
Ag3280
ppb
541.8
1.609
.297
Ca3179
ppb
454100.
2209
.4865
Fe2714
ppb
177600.
514.5
.2897
Na3302
PPB
5.527
.1759
3.183
1960-1
ppb
551.8
7.606
1.378
Ti3349
ppb
500.6
1.02
.2038
A13082
ppb
509500.
4246
.8334
Cd2265
ppb
477.5
2.125
.4451
K.7664
PPffl
Q25.60
.1305
.51
Ni2316
ppb
460.9
1.687
.3659
1960-2
ppb
532.9
10.46
1.963
T11908
ppb
511.6
8.779
1.716
Asl890
ppb
531.8
3.326
.6254
Ce4186
ppb"
502.3
2.045
.4072
Li6707
ppb
633.7
4.073
.6426
P.2149
ppb
533.4
.7771
.1457
Pb2203
ppb
494.4
3.804
.7695
V.2924
ppb
499.3
2.159
.4324
B.2496
ppb
526.6
1.098
.2085
C02286
ppb
479.3
1.418
.2959
Mg2790
ppb
533100.
742.1
.1392
2203-1
PPb
517.8
3.61
.6971
Sel960
PPb
539.2
4.675
.867
Zn2062
ppb
455.7
4.122
.9045
834934
ppb
519,8.
1.855
.3569
Cr2677
ppb
484.2
2.484
.513
Hn2576
ppb
465.3
1.645
.3531
2203-2
ppb
482.7
7.505
1.555
Snl399
ppb
519.4
5.933
1.142
S12S81
ppb
Q561.2
.1655
.0295
Be3130
ppb
501.4
2.35
.4686
CU3247
ppb
541.8
4.08
.7532
H02020
ppb
503.6
3.171
.6297
SD2068
ppb
541.0
4.554
.8419
Sr4215
ppb
514.1
1.336
.2598
252
-------
Analysis Report Averages
Ned 10-08-97 07:03:45 AH page 11
Method: TRIANGL2 Sanple Kane: 183-3-3B XSO Operator: OKH
Run Tiee: 10/08/97 03:13 filename: 100797
Hode: CONC Type: S Corr. Factor: 1.00000
Lab ID.: Cost. Snpl. ID.: Cust. ID.: 43231
Elens
Units
Avge
SDev
*RSD
Ag3280
ppb
1.044
.1188
11.38
Asl890
ppb
L2.S03
1.52
60.73
Ba4934
ppb
5.520
.0374
.6779
Be3130
ppb
L-.4856
.1021
21.03
Cd2265
ppb
5.922
.0996
1.682
C02286
ppb
1.1913
.2462
128.8
Eleras
Units
Avge
SDev
IRSD
Cr2677 Mn2576 Ni2316 P.2149 Pb2203 Sb2068
ppb ppb ppb' ppb ppb ppb
3.314 275.1 LI. 425 L9.324 314.2 L-.7330
.3705 .8535 .2619 6.96 1.483 2.275
11.18 .3103 18.37 74.64 .4721 310.3
Elens
Units
Avge
SDev
*RSD
Sel960
ppb
L-.2995
.8252
275.5
T11908 Zn2062
ppb ppb
L-4.121 1695.
4.451 9.086
108 .536
253
-------
Analysts Report Averages
Hed 10-08-97 07:03:45 AH page 12
Method: TRIAN6L2 Sainple Name: 183-3-3B X50 DA Operator: DKH
Run Tine: 10/08/97 03:17 Filenaae: 100797
Node: CONC Type: S Corr. Factor: 1.00000
Lab 10.: Cust. Snpl. ID.: Cust. ID.: 43231
Eleos
Units
Avge
SOev
*RSD
Ag3280 AS1890 8a4934 Be3130 Cd226S Co2286
ppb ppb ppb ppb ppb ppb
L.9757 LI. 265 5.506 L-.5472 6.065 L.1159
.1277 1.499 .0169 .0853 .1137 .472
13.09 118.5 .3076 15.59 1.874 407.4
Elems
Units
Avge
SDev
%RSD
Cr2677
ppb
3.396
.0287
.8445
Hn2576
ppb
275.2
.1284
.0466
N12316
Ppb"
LI. 512
.1862
12.32
P.2149
ppb
110.16
2.719
26.75
Pb2203
ppb
312.5
1.139
.3645
S52068
ppb
L.3145
.9085
288.9
El ens
Units
Avge
SDev
IRSD
Sel960
ppb
L.6587
1.008
153
T11908
ppb
L-.5729
2.393
417.6
Zn2062
ppb
1701.
6.754
.397
254
-------
Analysis Report Averages
led 10-08-97 07:03:45 AH page 13
Method: TRIANGL2 Sanple Naue: 183-3-SBC Operator: DKH
Run Tiae: 10/08/97 03:22 Filename: 100797
Node: CONC Type: S Corr. Factor: 1.00000
Lab ID.: Cust. Snpl. ID.: Cust. ID.: 43231
Elens
Units
Avge
SDev
«SD
Ag3280 As 1890 8a4934 8e3130 Cd2265 Co2286
ppb ppb ppb ppb ppb ppb
L.4457 L-2.903 2.443 L-.6678 1.853 L-1.064
.551 1.387 .0193 .0861 .0232 .2394
123.6 47.79 .7908 12.9 1.253 22.49
Eleins
Units
Avge
SDev
IRSD
Cr2677 Mn2576 Hi2316 P.2149 Pb2203 Sb2068
ppb ppb ppb* ppb ppb ppb
4.299 9.713 L-.8869 45.67 21.07 L.4292
.2999 .0352 .291 2.697 .4124 1.948
6.977 .3625 32.81 5.906 1.957 453.9
El BUS
Units
Avge
SDev
%RSD
Sel960
PPb
12.21
1.489
12.19
T11908
ppb
1-9.163
2.242
24.46
Zn2062
ppb
119.9
.933
.778
255
-------
.Analysie Report Averages
Ned 10-08-97 07:03:45 AH page 14
Method: TRIANGL2 Sanple Name: 183-3-6C Operator: DKH
Run Tine: 10/08/97 03:27 Filenane: 100797
Node: COHC Type: S Corr. Factor: 1.00000
Lab ID.: Cust. Supl. ID.: Cust. 10.: 43231
Eless
Units
Avge
SDev
*RSD
Ag3280 Asl890 Ba4934 Be3130 Cd2265 Co2286
ppb ppb ppb ppb ppb ppb
L.7462 L-3.814 3.063 L-.7413 1.053 L-1.179
.6181 1.747 .0374 .0963 .0361 .4345
82.84 45.8 1.222 12.99 3.427 36.84
Elems
Units
Avge
SOev
tRSD
Cr2677 Mn2576 Ni2316 P.2149 Pb2203 Sb2068
ppb ppb ppb* ppb ppb ppb
7.699 7.149 L.2620 86.70 16.76 LI. 291
.3404 .0241 .6199 3.035 1.009 2.165
4.421 .337 236.6 3.5 6.02 167.8
Elems
Units
Avge
SOev
IRSD
Sel960 T11908 2n2062
ppb ppb ppb
L.7528 L-10.08 119.2
1.169 2.541 1.505
155.3 25.21 1.263
256
-------
Analysis Report Averages
Ned 10-08-97 07:03:45 AH page 15
Method: TRIANGL2 Sanple Nane: 183-3-7C Operator: DKH
Run Tine: 10/08/97 03:31 Filenane: 100797
Mode: CQNC Type: S Corr. Factor: 1.00000
Lab ID.: Cust. Srapl. ID.: Cust. ID.: 43231
Elens
Units
Avge
SOev
*RSD
Ag3280 Asl890 Ba4934 Be3130 Cd2265 Co2286
ppb ppb ppb ppb ppb ppb
L.9317 1-3.666 7.064 L-.8442 L.8941 L-.7697
.2618 .6801 .0692 .0566 .2032 .4057
28.1 18.55 .9797 6.709 22.72 52.72
Elens
Units
Avge
SDev
*RSD
Cr2677 Nn2576 Ni2316 PJ149 Pb2203 Sb2068
ppb ppb ppb' ppb ppb ppb
9.822 8.633 LI. 456 107.6 21.37 L.2146
.783 .1202 .6213 6.923 .6768 2.654
7.972 1.393 42.68 6.432 3.168 1237
Elens
Units
Avge
SDev
mo
Sel960
ppb
14.20
1.198
8.437
T11908
ppb
L-7.985
1.925
24.11
Zn2062
ppb
154.9
1.426
.9203
257
-------
. Analysis Report Averages
tied 10-08-97 07:03:45 AH page 16
Method: TRIANGL2 Sample Name: 183-3-8C Operator: DKH
Run Tine: 10/08/97 03:36 Filename: 100797
Hode: CONC Type: S Corr. Factor: 1.00000
Lab ID.: Gust. Sinpl. ID.: Cust. ID.: 43231
El ens
Units
Avge
SDev
*RSD
Ag3280 Asl890 Ba4934 8e3130 Cd226S Co2286
ppb ppb ppb ppb ppb ppb
L.5251 L-3.138 3.658 L-.8049 L.6621 L-1.302
.5607 1.168 .0731 .0684 .0519 .6143
106.8 37.21 1.997 8.494 7.839 47.17
Elens
Units
Avge
SDev
%RSD
Cr2677 Mn2576 Ni2316 P.2149 Pb2203 Sb2068
ppb ppb ppb' ppb ppb ppb
8.300 16.37 8.018 111.5 24.25 L-.6075
.5082 .1623 1.394 .1818 1.223 1.192
6.124 .9914 17.39 .163 5.044 196.3
El ems
Units
Avge
SDev
%RSD
Sel960
ppb
LI. 416
.7877
55.65
T11908
ppb
1-9.210
2.172
23.58
Zn2062
PPb
143.9
1.707
1.186
258
-------
Analysis Report Averages
Ned 10-08-97 07:03:45 AH page 17
Method: TRIANGL2 Sanpie Nane: 43231 MB Operator: DKH
Run Tine: 10/08/97 03:41 Filenane: 100797
Node: CONC Type: S Corr. Factor: 1.00000
Lab ID.: Oust. Sapl. ID.: Cust. ID.: 43231
Elens
Units
Avge
SDev
*RSD
Ag3280 AS1890 Ba4934 Be3130 Cd226S Co2286
ppb ppb ppb ppb ppb ppb
L-.0396 L-1.678 L-.0358 L-.8093 L-.244.3 L-.5261
.1657 2.249 .0228 .0378 .0286 .1993
419 134 63.59 4.668 11.71 37.89
Elens
Units
Avge
SDev
*RSD
Cr2677
Ppb
L.0685
.1353
197.5
Hn2576
ppb
2.844
.0327
1.149
H12316
ppb-
L-1.131
.8425
74.48
P.2149
ppb
1-13.83
5.068
36.64
Pb2203
ppb
LI. 672
1.382
82.69
Sb2068
PPb
L-.8198
.1904
23.23
Eleos
Units
Avge
SOev
%RSD
Sel960
ppb
L.2343
1.519
648.4
TH908
PPb
L-5.424
3.046
56.16
Zn2062
ppb
9.791
.3881
3.964
259
-------
Analysis Report Averages
Red 10-08-97 07:03:45 AH page 18
Method: TRIAN6L2 Saaple Name: 43231 LCS Operator: DKH
Run Tine: 10/08/97 03:45 Filename: 100797
Node: CONC Type: S Corr. Factor: 1.00000
Lab ID.: Cust. Sipl. ID.: Oust. ID.: 43231
Elens
Units
Avge
SDev
IRSO
Ag3280 As 1890 Ba4934 Be3130 Cd2265 Co2286
ppb ppb ppb ppb ppb ppb
43.16 44.64 46.44 45.27 45.89 46.96
.5728 2.289 .0724 .212 .1659 .7293
1.327 5.129 .1559 .4684 .3616 1.553
Elens
Units
Avge
SDev
IRSD
Cr2677 Hn2576 Hi2316 P.2149 Pb2203 Sb2068
ppb ppb ppb' ppb ppb ppb
46.87 47.66 45.34 904.6 46.69 47.00
.5382 .2079 .9026 4.625 .419 2.523
1.148 .4362 1.991 .5112 .8974 5.368
Elens
Units
Avge
SDev
IRSO
Sel960
ppb
44.37
1.676
3.777
T11908
ppb
41.73
5.652
13.54
Zn2062
ppb
192.4
1.968
1.023
260
-------
Analvsis fteoort. Averaoes
Ued 10-22-97 03:23:25 PH page SO
Method: TRIANG12 Sanole Nw>: 184-23-IA8 X50 Operator: OKH
Run TiiB: 10/08/97 03:SO filename: 100797
Mnrtp- COW Type: s Corr. Factor: 1.00000
l.ah Ff>.: i:nsf. Snnl. ID.: Cust. fO.: 43231
FlRRS
llni ts
Avae
SOev
tRSO
Aa3?80
ppb
2.106
.2924
13.88
A* 1890
ppb
29.07
1.681
5.781
Ra4934
PPb
281.0
.5952
.2118
8e?l30
ppb
I -.4995
.0279
5.586
M2265
ppb
271:5
1.224
.4507
Cr2677
ppb
244.8
1.562
.638
El ens
Units
Avge
SDev
4RSD
Mn2576
ppb
15900.
48.69
.3063
N12316
ppb
56.60
.2706
.4782
Sb2068
PPb"
163.0
3.625
2.224
Pb2203
ppb
15620.
40.79
.2611
S61960
ppb
14.83
.8455
5.703
P.2149
PPb
356.3
9.271
2.602
llni ts
Avap
PPb
HVI.',RO.
505.5
.70Ss
261
-------
•Analysis Report Averages
Ned 10-22-97 03:23:25 PH page 51
ItRt.M: TRTANG1.2 Sannle Naie: 184-23-2AB X50 Operator: DKH
Run Tine: 10/08/97 03:55 Filenane: 100797
Mode: COHC Tvp«: S Corr. Factor: 1.00000
Lab 10.: Ciist. Snipl. ID.: Cust. 10.: 43231
iinirs
HVOP
Sfmv
tHSf
Hems
Unit.?
Avge
SOev
iRSO
El eras
Units
Avae
SOev
SRSD
Ao3?RO
ppb
3. 97ft
2115
S.32
Hn257h
ppb
H37240.
9S.42
.2563
Zn2062
ppb
HI 79200.
958.6
.5349
As 1890
onh
51.li
.4.VS
.RSI 2
Hi 2316
ppb
91.50
.12R6
.1406
ppb ppb
560.7 2.29^
1.436 .0471
Pb2203
ppb
38770.
134.)
.3458
Sb2068
ppb
286.0
3.869
1.353
ppb
737:2
1.865
.25?<»
Sel%0
ppb
21.79
3.714
17.04
Cr2677
ppb
477.8
1.329
.2782
P.2149
ppb
584.0
6.085
1.042
262
-------
• Analysis Report Averages
Wed 10-08-97 07:03:45 AH page 23
Method: TRIANGL2 Sample Name: ICV/CCV Operator: DKH
Run Tine: 10/08/97 04:14 Filename: 100797
Mode: CONC Type: 0 Corr. Factor: 1.00000
Lab ID.: Cust. Sipl. ID.: Cust. ID.: 43231
Elens
Units
Avge
SOev
IRSD
eiems
Units
Avge
SOev
*RSD
Elens
Units
Avge
SOev
*RSD
Eleas
Units
Avge
SOev
USD
El ems
Units
Avge
SDev
*RSD
Elems
Units
Avge
SDev
tRSD
Ag3280
ppb
517.9
4.507
.8703
Ca3179
ppb
513.9
1.302
.2534
Fe2714
ppb
514.6
6.603
1.283
N33302
PP»
5.187
.204
3.932
1960-1
PPb
523.3
6.133
1.172
Ti3349
PPb
501.5
.5115
.102
A13082
ppb
460.7
18.55 .
4.026
Cd2265
ppb
505.6
.883
.1746
KJ664
ppm
5.130
.0308
.5996
Ni2316
ppb
504.0
1.02
.2023
1960-2
PPb
517.6
.7649
.1478
T11908
PPb
514.0
14.4
2.801
AS1890
ppb
517.2
1.425
.2756
Ce4186
PPb'
501.8
.6708
.1337
Li6707
PPb
496.9
3.029
.6096
P.2149
ppb
518.3
3.507
.6766
Pb2203
PPb
509.2
1.529
.3003
V.2924
PPb
513.0
.6666
.1299
8.2496
ppb
506.6
1.399
.2762
C02286
ppb
516.4
1.013
.1961
«g2790
PPb
510.8
6.294
1.232
2203-1
PPb
515.5
5.643
1.095
Sel960
PPb
519.5
1.557
.2997
Zn2062
ppb
520.2
1.145
.2202
8a4934
PPb
505.5
1.147
.2269
Cr2677
PPb
509.7
1.124
.2204
Mn2576
PPb
507.2
1.056
.2081
2203-2
PPb
506.0
4.409
.8714
Snl899
PPb
509.7
1.421
.2789
512881
PPb
Q4031.
40.92
1.015
Be3130
ppb
520.7
1.784
.3427
CU3247
ppb
506.5
4.846
.9567
M02020
PPb
510.8
.8218
.1609
Sb2068
ppb
488.5
6.627
1.356
Sr4215
PPb
500.8
.6648
.1327
263
-------
.Analysis Report Averages
Wed 10-08-97 07:03:45 AN page 24
Method: TRIANGL2 Sample Name: ICB/CC8 Operator: OKH
Run Time: 10/08/97 04:21 Filename: 100797
Mode: CONC Type: Q Corr. Factor: 1.00000.
Lab ID.: Cust. Snpl. ID.: Cust. ID.: 43231
Eleas
Units
Avge
SDev
*RSD
Elens
Units
Avge
SDev
*RSD
El ems
Units
Avge
SDev
%RSD
Elems
Units
Avge
SDev
%RSD
Elems
Units
Avge
SDev
IRSD
Elens
Units
Avge
SDev
IRSD
Ag3280
ppb
.3128
.3591
114.8
Ca3179
ppb
3.224
.5812
18.03
Fe2714
ppb
-1.564
4.462
285.3
Na3302
ppm
.0201
.0566
281
1960-1
ppb
1.335
4.77
357.3
Ti3349
ppb
.2912
.0837
28.74
A13082
ppb
Q-55.57
10.97
19.74
Cd2265
ppb
.3109
.0926
29.8
K.7664
ppro
.0383
.026
67.84
N12316
ppb
.7390
.4273
57.82
1960-2
ppb
-3.378
1.336
39.55
T11908
ppb
1.979
.7565
38.24
As 18<50
ppb
2.068
1.174
56.77
Ce4186
PPb"
-.4351
.9053
208.1
Li6707
ppb
.3578
.0314
8.78
P.2149
ppb
.8917
7.335
822.6
Pb2203
ppb
-.3417
1.369
400.8
V.2924
ppb
-.2019
.3413
169
8.2496
ppb
-2.761
1.116
40.43
Co2286
ppb
.5022
.031
6.182
Hg2790
ppb
-2.137
.3262
15.26
2203-1
ppb
-1.575
3.249
206.4
Sel960
ppb
-1.809
2.419
133.7
Zn2062
ppb
1.549
.3892
25.14
Ba4934
ppb
.2773.
.0693
24.98
Cr2677
PPb
-.0139
.2684
1932
Mn2576
ppb
.5610
.1751
31.21
2203-2
ppb
.2739
.4365
159.4
Snl899
PPb
.6920
.957
138.3
Si2881
ppb
9.747
3.493
35.83
Be3130
ppb
-.5910
.188
31.81
Cu3247
ppb
.8741
.4261
48.74
N02020
pob
.0916
.2306
251.6
Sb2068
PPb
2.822
1.423
50.44
Sr4215
ppb
.2953
.0741
25.1
264
-------
.Analysis Report Averages Ned 10-08-97 07:03:45 AH page 25
Method: TRIAN6L2 Saiple Name: 1B4-23-1A8 X200 Operator: DKH
Run Tine: 10/08/97 04:26 Filenaae: 100797
Node: CONC Type: S Corr. Factor: 1.00000
Lab ID.: Cust. Supl. ID.: Oust. ID.: 43231
Elens
Units
Avge
SOev
*RSD
Ag3280 Asl890 8a4934 Be3130 Cd2265 C02286
ppb ppb ppb ppb ppb ppb
L.7194 9.565 72.20 L-.7956 70.37 1.860
.3148 1.313 .4395 .084 .3039" .2726
43.75 13.73 .6087 10.56 .4319 14.66
Eleus
Units
Avge
SOev
*RSD
Cr2677 Nn2576 Ni2316 P.2149 Pb2203 Sb2068
ppb ppb ppb- ppb ppb ppb
63.44 4246. 15.61 92.21 4059. 43.64
.2711 9.774 .2253 7.586 11.67 1.385
.4274 .2302 1.443 8.227 .2875 3.174
Elens Sel960 T11908 Zn2062
Units ppb ppb ppb
Avge L2.392 LI.165 19590.
SDev 2.038 1.445 133.7
*RSD 85.17 124 .6826
265
-------
Analysis Report Averages Ned 10-08-97 07:03:45 AN page 26
Method: TRIANGL2 Sample Naae: 184-23-2A8 X200 Operator: DKH
Run Tine: 10/08/97 04:31 Filename: 100797
Hode: CONC Type: S Corr. Factor: 1.00000
Lab ID.: Oust. Sopl. ID.: Cust. ID.: 43231
Elens
Units
Avge
SDev
tRSD
Ag3280 Asl890 8a4934 Be3130 Cd2265 Co2286
ppb ppb ppb ppb ppb ppb
L.9297 15.16 143.3 L-.1602 191,9 2.426
.1652 .9641 .5275 .0517 .7189 .2134
17.77 6.36 .3681 32.31 .3747 8.795
Eleins
Units
Avge
SDev
*RSD
Cr2677 Mn2576 Hi2316 P.2149 Pb2203 Sb2068
ppb ppb ppb' ppb ppb ppb
123.1 10530. 24.49 150.6 10050. 73.48
.3161 25.72 .4927 .7415 25.17 1.203
.2568 .2441 2.012 .4922 .2503 1.637
El ens
Units
Avge
SDev
mo
Sel960 T11908 Zn2062
ppb ppb ppb
4.951 7.234 56240.
1.055 2.025 399.3
21.32 28 .7099
266
-------
Analysis Report Averages Wed 10-08-97 07:03:45 AH page 27
Method: TRIANGL2 Saople Naie: 184-23-2AB X200 L Operator: DKH
tun Tine: 10/08/97 04:36 Filename: 100797
.lode: COHC Type: S Corr. Factor: 1.00000
Lab 10.: Cust. Sopl. ID.: Cust. ID.: 43231
Eleis
Units
ivge
JDev
*RSD
Ag3280 Asl890 Ba4934 Be3130 Cd2265 Co2286
ppb ppb ppb ppb ppb ppb
L.1229 6.008 29.30 L-.8341 39.4? L.4516
.2684 .4912 .0327 .0684 .1391 .3627
218.3 8.176 .1116 8.202 .3522 80.31
ileis
Units
^vge
!Dev
*RSD
Cr2677
ppb
24.93
.4886
1.96
Mn2576
ppb
2214.
7.977
.3603
Ni2316
ppb-
5.732
.7371
12.86
P.2149
ppb
33.61
1.725
5.133
Pb2203
ppb
2069.
6.866
.3319
Sb2068
ppb
15.78
.6887
4.364
ilens Sel960 111908 Zn2062
Units ppb ppb ppb
Avge 1.4343 LI.873 12160.
iOev 1.085 .7286 79.66
JRSD 249.5 38.9 .6551
267
-------
•Analysis Report Averages Ned 10-08-97 07:03:45 AM page 28
Method: TRIANGL2 Sample Name: 184-23-3AB X200 Operator: DKH
Run Tine: 10/08/97 04:40 Filenane: 100797
Node: COHC Type: S Corr. Factor: 1.00000
Lab ID.: Cust. Sipl. ID.: Cust. ID.: 43231
Elens
Units
Avge
SDev
IRSD
Ag3280 Asl890 Ba4934 Be3130 Cd2265 Co2286
ppb ppb ppb ppb ppb ppb
L.6353 15.68 124.8 L-.5840 150.5 2.487
.2422 1.31 .4022 .0355 .8995 .4445
38.12 8.355 .3223 6.079 .5975. 17.87
Elems
Units
Avge
SDev
*RSD
Cr2677
ppb
101.7
.9317
.9157
Hn2576
ppb
8286.
40.56
.4895
Ni2316
ppb'
24.91
.4901
1.967
P.2149
ppb
3054.
10.03
.3284
Pb2203
ppb
7390.
47.67
.6451
Sb2068
ppb
64.67
1.253
1.937
Elens
Units
Avge
SDev
*RSD
Sel960
PPb
4.709
1.534
32.57
T11908
PPb
5.921
1.674
28.27
Zn2062
ppb
38710.
381.9
.9866
268
-------
, Analysis Report Averages
Ned 10-08-97 07:03:45 AH page 29
Method: TRIANGL2 Sanple Nane: 184-23-3A8 X200 PA Operator: DXH
Run Tine: 10/08/97 04:47 Filenaue: 100797
Mode: CONC Type: S Corr. Factor: 1.00000
Lab ID.: Cust. Sipl. ID.: Cust. ID.: 43231
Elens
Units
Avge
SDev
*RSD
Elens
Units
Avge
SDev
IRSD
Elens
Units
Avge
SDev
*RSD
Ag3280
ppb
L.8864
.1601
18.06
Cr2677
ppb
104.1
.6927
.6653
Sel960
ppb
6.213
.2846
4.581
AS1890
Ppb
17.30
1.648
9.526
Hn2576
ppb
8430.
47.33
.5615
T11908
ppb
L3.271
2.775
84.85
8a4934
ppb
127.0
.3263
.2569
N12316
ppb'
25.63
.4261
1.662
Zn2062
PPb
39480.
440.8
1.117
8e3130
ppb
L-.5885
.0714
12.14
PJ149
ppb
3137.
4.917
.1567
Cd2265
ppb
153,5
.7414
.483
Pb2203
ppb
7544.
51
.676
Co2286
ppb
3.318
.4442
13.38
SD2068
ppb
68.21
1.216
1.783
-------
> Analysis Report Averages
Ned 10-08-97 07:03:45 AN page 30
Method: TRIANGL2 Sample Nane: 184-23-4AB Operator: DKH
Run Tine: 10/08/97 05:01 Filenaae: 100797
Node: CONC Type: S Corr. Factor: 1.00000
Lab ID.: Cust. Sopl. ID.: Cust. ID.: 43231
Eleas
Units
Avge
SDev
IRSD
Ag3280
ppb
66.89
.7716
1.154
AS1890
ppb
32.62
2.77
8.49
Ba4934
ppb
498.7
.9166
.1838
8e3130
ppb
L-51.18
.1834
.3584
Cd2265
ppb
1692,
8.242
.4871
C02286
ppb
35.48
1.033
2.911
Eleos
Units
Avge
SDev
USD
Cr2677
ppb
319.3
1.052
.3295
Nn2576
ppb
336.8
.8933
.2652
Ni2316
ppb'
180.9
.5335
.2948
P.2149
ppb
1252.
6.946
.5549
Pb2203
ppb
5839.
46.04
.7885
Sb2068
ppb
47.57
2.725
5.728
Eleus
Units
Avge
SDev
*RSD
Sel960
ppb
40.79
2.281
5.593
T11908
ppb
L-6.404
3.978
62.11
Zn2062
ppb
1619.
12.64
.7807
270
-------
•Analysis Report Averages
Med 10-08-97 07:03:45 AH page 31
Method: TRIANGL2 Sample Nane: 184-23-6AB Operator: DXK
Run Tine: 10/08/97 05:14 Filename: 100797
Mode: CONC Type: S Core. Factor: 1.00000
Lab ID.: Cust. Snpl. ID.: Cust. ID.: 43231
Eleois
Units
Avge
SOev
*RSD
Ag3280
PPb
3.703
.417
11.26
As 1890
ppb
9.119
.6883
7.548
834934
PPb
640.5
2.817
.4398
Be 3 130
ppb
1-1.231
.1135
9.22
Cd2265
PPb
349,6
3.283
.9392
C02286
ppb
1-24.98
1.177
4.713
Eleois
Units
Avge
SDev
%RSD
Cr2677
ppb
99.38
1.763
1.774
Mn2576
ppb
394.0
2.922
.7416
Ni2316
ppb"
64.69
1.515
2.343
PJ149
PPb
905.6
13.26
1.465
Pb2203
PPb
1789.
21.76
1.216
Sb2068
PPb
54.73
7.679
14.03
Elenis
Units
Avge
SDev
IRSD
Sel960
PPb
48.29
1.461
3.026
T11908 2n2062
PPb ppb
1-37.40 1532.
4.864 27.83
13 1.816
271
-------
•Analysis Report Averages
Med 10-08-97 07:03:45 AN page 32
Method: TRIANGL2 Sample Name: 184-23-7A8 Operator: DKH
Run Tine: 10/08/97 05:22 Filename: 100797
Node: CONC Type: S Corr. Factor: 1.00000
Lab 10.: Cust. Sipl. ID.: Oust. ID.: 43231
Eleus
Units
Avge
SDev
tRSD
Ag3280 Asl890 Ba4934 8e3130 Cd2265 Co2286
ppb ppb ppb ppb ppb ppb
3.501 8.426 635.8 1-1.212 9.254 L-25.88
.4752 1.632 3.038 .0923 .506 1.322
13.57 19.37 .4779 7.616 5.468 5.111
Eleos
Units
Avge
SDev
IRSO
Cr2677 Nn2576 Ni2316 P.2149 Pb2203 Sb2068
ppb ppb ppb' ppb ppb ppb
93.83 550.6 58.20 810.3 404.0 55.62
2.26 4.139 2.158 10.63 2.931 4.187
2.409 .7518 3.708 1.312 .7254 7.528
El eras
Units
Avge
SOev
tRSD
Sel960 111908 Zn2062
ppb ppb ppb
48.53 L-36.83 2495.
2.15 6.274 43.83
4.43 17.04 1.757
272
-------
Analysis Report Averages
Ned 10-08-97 07:03:45 AN page 33
Method: TR1ANGL2 Sample Name: 184-23-8A8 Operator: DKH
Run Tine: 10/08/97 05:32 Filename: 100797
Node: CONC Type: S Corr. Factor: 1.00000
lab ID.: Cust. Sspl. ID.: Cust. ID.: 43231
Eleos
Units
Avge
SDev
IRSD
Ag3280
ppb
8.771
.7565
8.625
Asl890
ppb
10.13
4.634
45.73
Ba4934
ppb
672.5
3.113
.4629
Be3130
ppb
L-1.286
.0941
7.317
Cd2265
ppb
102.2
1.213
1.186
Co2286
ppb
L-27.12
1.247
4.598
Eleras
Units
Avge
SDev
*RSD
Cr2677
ppb
107.5
2.244
2.088
Mn2576
ppb
920.2
5.867
.6375
N12316
PPb"
64.98
2.023
3.114
PJ149
ppb
708.1
11.84
1.672
Pb2203
ppb
943.6
7.653
.811
Sb2068
ppb
60.84
5.1
8.383
Eleras
Units
Avge
SDev
USD
Sel960
ppb
52.38
4.894
9.342
T11908 Zn2062
ppb ppb
L-37.50 5842.
4.205 86.33
11.21 1.478
273
-------
Analysis'Report Averages
Ned 10-08-97 07:03:45 All page 34
Hethod: TRIANGL2 Sample Name: ICV/CCV Operator: OKH
Run Tine: 10/08/97 05:40 Filename: 100797
Node: CONC Type: Q Corr. Factor: 1.00000
Lab ID.: Oust. Sopi. ID.: Cust. ID.: 43231
Elems
Units
Avge
SDev
IRSO
Elens
Units
Avge
SDev
%RSD
Eleras
Units
Avge
SDev
%RSD
El eras
Units
Avge
SDev
%RSD
Eleos
Units
Avge
SDev
IRSD
Eleos
Units
Avge
SDev
IRSD
Ag3280
ppb
512.8
2.075
.4045
Ca3179
ppb
508.1
4.888
.9622
Fe2714
ppb
505.5
13.94
2.758
Na3302
ppra
5.139
.0783
1.524
1960-1
PPb
522.6
4.038
.7726
T13349
ppb
495.1
1.193
.2411
A13082
ppb
Q434.7
17.43
4.01
Cd2265
ppb
497.1
3.6
.7242
K.7664
ppffl
5.094
.0235
.4614
N12316
ppb
498.7
2.831
.5677
1960-2
ppb
508.1
3.688
.7257
TH908
ppb
506.0
13.35
2.639
As 1890
ppb
512.8
2.122
.4139
Ce4186
ppb'
496.9
2.988
.6012
LJ6707
ppb
495.0
2.076
.4194
P.2149
ppb
513.5
5.308
1.034
Pb2203
ppb
495.4
3.945
.7963
V.2924
ppb
512.4
2.89
.564
8.2496
ppb
3610.
425
11.77
Co2286
ppb
514.0
3.626
.7054
Mg2790
ppb
505.7
5.241
1.036
2203-1
ppb.
512.1
5.822
1.137
Sel960
ppb
513.0
2.916
.5684
Zn2062
ppb
511.0
7.061
1.382
8a4934
ppb
504,0
2.289
.4542
Cr2677
ppb
507.4
4.47
.881
Mn2576
ppb
505.0
2.909
.576
2203-2
ppb
487.1
7.439
1.527
Snl899
ppb
503.3
4.294
.8532
S12881
ppb
059310.
3810
6.423
8e3130
ppb
525.4
3.864
.7354
Cu3247
ppb
504.9
4.972
.9848
No2020
ppb
506.5
3.03
.5982
Sb2068
ppb
485.8
6.261
1.289
Sr4215
ppb
500.4
1.525
.3048
274
-------
.Analysis Report Averages
Ned 10-08-97 07:03:45 AN page 37
Method: TRIANGL2 Sample Name: ICB/CC8 Operator: DKH
Run Time: 10/08/97 06:06 Filenane: 100797
Node: CONC Type: Q Corr. Factor: 1.00000
Lab ID.: Cust. Snpl. ID.: Cust. ID.: 43231
Elens
Units
Avge
SDev
*RSD
Elens
Units
Avge
SDev
USD
Elens
Units
Avge
SDev
USD
El ems
Units
Avge
SDev
USD
Elens
Units
Avge
SDev
USD
Elens
Units
Avge
SDev
USD
Ag3280
ppb
.2309
.5822
252.1
Ca3179
ppb
.3246
1.112
342.5
Fe2714
ppb
-.8432
9.396
1114
Na3302
ppin
.0906
.0971
107.2
1960-1
ppb
5.736
2.575
44.89
Ti3349
ppb
-.1543
.1032
66.87
A13082
ppb
Q-53.89
8.679
16.11
Cd2265
ppb
.7877
.0724
9.186
KJ664
ppn
.0036
.0403
1114
N12316
ppb
-.1408
.1854
131.7
1960-2
ppb
-1.977
.6189
31.3
T11908
ppb
-.8034
.9901
123.2
AS1890
ppb
2.654
2.048
77.17
Ce4186
PPb"
.6887
1.897
275.5
Li6707
ppb
-.1073
.0846
78.76
P.2149
ppb
3.792
7.114
187.6
Pb2203
ppb
-.0061
2.035
33330
V.2924
ppb
-.9228
.6983
75.67
B.2496
ppb
2256.
158.8
7.037
C02286
ppb
-.2525
.6182
244.8
Hg2790
ppb
-3.960
3.642
91.99
2203-1
ppb
-.8636
3.54
409.9
Sel960
PPb
.5911
.6391
108.1
2n2062
PPb
-.3258
.1348
41.38
8a4934
ppb
-.0779
.0367
47.14
Cr2677
ppb
.0688
.5652
821.5
Mn2576
ppb
-.0765
.0157
20.56
2203-2
ppb
.4220
1.571
372.2
Snl899
ppb
-1.153
.2231
19.34
S12881
ppb
06815.
1692
24.82
8e3130
ppb
-.9839
.0908
9.226
Cu3247
ppb
.0251
.1111
443.5
1402020
ppb
-.7988
.1386
17.35
Sb2063
ppb
-1.775
2.381
134.2
Sr4215
ppb
-.0681
.0303
44.45
2-75
-------
'Analysis Report Averages
Hed 10-08-97 07:03:45 AH page 38
Method: TRIANGL2 Sample Naae: 184-23-9A8 Operator: DKH
Run Time: 10/08/97 06:11 Filename: 100797
Mode: COHC Type: S Corr. Factor: 1.00000
Lab ID.: Cust. Snpl. ID.: Cust. ID.: 43231
Elegs
Units
Avge
SDev
USD
Ag3280
ppb
1.896
.4018
21.19
Asl890
ppb
15.11
3.117
20.63
Ba4934
ppb
622.4
2.207
.3546
863130
ppb
L-1.061
.0619
5.83
Cd2265
ppb
L-6.618
.3033
4.542
C02286
ppb
L-23.92
.6385
2.669
Eleas
Units
Avge
SDev
%RSD
Cr2677 Nn2576 Hi2316 P.2149 Pb2203 Sb2068
ppb ppb ppb' ppb ppb ppb
92.61 26.98 59.94 786.7 L-.9452 60.11
1.197 .2808 .6297 7.513 .5112 5.605
1.293 1.041 1.05 .955 54.08 9.325
Eless
Units
Avge
SDev
*RSD
Sel960
ppb
51.48
1.433
2.785
T11908
ppb
L-41.02
2.863
6.979
Zn2062
ppb
51.73
1.489
2.878
276
-------
Analysis'Report Averages
Hed 10-08-97 07:03:45 AH page 39
Method: TRIANGL2 Sample Naae: 184-23-10AB.5 Operator: DKH
Run Tine: 10/08/97 06:20 Filenaae: 100797
Mods: COHC Type: S Corr. Factor: 1.00000
Lab ID.: Cust. Snpl. ID.: Cust. ID.: 43231
Elees
Units
Avge
SOev
*RSD
Ag3280 As 1890 Ba4934 8e3130 Cd2265 Co2286
ppb ppb ppb ppb ppb ppb
3.105 33.47 1035. L-55.53 L-6.7Q6 27.75
.707 5.345 5.434 .4368 .161 1.328
22.77 15.97 .5249 .7866 2.401 4.786
Eleos
Units
Avge
SDev
IRSD
Cr2677
PPb
402.9
5.14
1.276
Hn2576
ppb
239.7
1.855
.7739
N12316
ppb"
158.1
1.882
1.19
PJ149
ppb
788.1
13.88
1.761
Pb2203
ppb
57.98
2.485
4.287
Sb2068
ppb
69.89
6.015
8.607
El ems
Units
Avge
SDev
%RSD
Sel960 T11908 Zn2062
ppb ppb ppb
60.90 1-15.12 564.6
1.602 9.699 11.02
2.631 64.13 1.952
2-71
-------
•Analysis Report Averages
Wed 10-08-97 07:03:45 AH page 40
Method: TRIANGL2 Sample Nane: 183-1S-1C Operator: DKH
Run Tine: 10/08/97 06:25 Filename: 100797
Node: CONC Type: S Corr. Factor: 1.00000
Lab ID.: Cust. Sapl. ID.: Cust. ID.: 43231
Elens
Units
Avge
SDev
IRSD
Ag3280 AS1890 8a4934 Be3130 Cd2265 Co2286
ppb ppb ppb ppb ppb ppb
L.5711 7.872 3.212 L-1.241 L-.8955 L-3.361
.3791 3.012 .0806 .0341 .1938 .2172
66.38 38.26 2.509 2.746 21.64 6.464
Eleas
Units
Avge
SDev
IRSD
Cr2677
ppb
13.98
1.376
9.837
Hn2576
ppb
3.676
.031
.8445
Ni2316
PPb'
8.472
.8*048
9.499
P.2149
ppb
L2.904
4.614
158.9
Pb2203
PPb
L.4317
1.306
302.6
Sb2068
ppb
4.816
2.022
41.99
[less
Units
Avge
SDev
%RSD
Sel960 T11908 Zn2062
ppb ppb ppb
8.973 1-10.79 12.31
1.557 2.52 .3826
17.35 23.36 3.107
273
-------
••Analysis Report Averages
Ned 10-08-97 07:03:45 AH page 41
Method: TRIANGL2 Sample Nane: ICV/CCV Operator: DKH
Run Tine: 10/08/97 06:29 Filename: 100797
Node: CONC Type: 0 Corr. Factor: 1.00000
Lab ID.: Cust. Snpl. ID.: Oust. ID.: 43231
El ems
Units
Avge
SOev
USD
Eleos
Units
Avge
SDev
USD
El ems
Units
Avge
SDev
USD
Eleras
Units
Avge
SDev
USD
Elenis
Units
Avge
SDev
USD
Elems
Units
Avge
SDev
USD
Ag3280 A13082
ppb ppb
0341*9
AS1890
ppb
8348.8
C42265
ppb
0332.3
287.8
86.59
Ca3179
ppb
0390.3
321.7
82.42
Ce4186
ppb-
324.6
280.8
86.5
C02286
ppb
0335.6
290
86.4
Li6707
ppb
0327.7
282.1
86.08
K.7664
ppm
03.664
2.417
65.97
Ni2316
ppb
0333.5
285.7
85.67
Fe2714
ppb
0256.3
247.9
96.69
Na3302
ppm
03.351
3.109
92.78
1960-1
ppb
320.5
271.6
84.74
Pb2203
PPb
0316.8
277
87.41
2203-1
PPb
301.5
276
91.56
Sel960
ppb
0331.0
286.9
86.66
H3349 T11908 V.2924
ppb . ' ppb ppb
0328.6 0342.4 0340 .J^
284.^4 - Mfcr— 78O
86.56 85.24 84.79
8e3130
PPb
0345.4
301.9
87.41
CU3247
-------
"Analysis Report Averages
Red 10-08-97 07:03:45 AH page 42
Method: TRIAN6L2 Sample Name: 183-15-lB/W-z^ju. Operator: OKH
Run Time: 10/08/97 06:34 Filename: 100797
Mode: CONC Type: S Corr. Factor: 1.00000
Lab ID.: Oust. Sspl. ID.: Cust. ID.: 43231
El ens
Units
Avge
SDev
IRSD
Ag3280 AS1890 Ba4934 8e3130 Cd226S Co2286
ppb ppb ppb ppb ppb ppb
1.186 1-4.801 4.324 L-.9855 L-1.092 L-4.620
.6274 4.186 .0528 .1946 1.363 3.53
52.91 87.2 1.221 19.74 124.8 76.41
Eleins
Units
Avge
SDev
%RSD
Cr2677
PPb
17.92
2.965
16.55
Nn2576
PPb
6.018
.2937
4.881
Ni2316
PPb'
5.207
3.437
66.01
P.2149
ppb
126.4
33.78
26.72
Pb2203
ppb
9.672
2.535
26.21
Sb2068
ppb
8.746
9.177
104.9
Eletos
Units
Avge
SDev
%RSD
Sel960
ppb
6.364
.3434
5.396
T11908
ppb
L-11.77
1.767
15.01
Zn2062
ppb
127.0
4.356
3.43
230
-------
> Analysis Report Averages
Ned 10-08-97 07:03:45 AN page 43
Method: TRIANGL2 Sample Name: ICV/CCV Operator: DKH
Run Tiie: 10/08/97 06:39 Filename: 100797
Node: CONC Type: Q Corr. Factor: 1.00000
Lab ID.: Cust. Srapl. ID.: Cust. ID.: 43231
Elens
Units
Avge
SOev
USD
Elens
Units
Avge
SOev
IRSD
Elens
Units
Avge
SOev
*RSD
Elens
Units
Avge
SDev
IRSD
Eleas
Units
Avge
SDev
%RSD
Elens
Units
Avge
SDev
*RSD
Ag3280
ppb
516.3
1.698
.329
Ca3179
ppb
509.7
.9727
.1908
Fe2714
ppb
507.8
4.159
.819
Na3302
ppn
5.205
.1597
3.068
1960-1
ppb
526.9
.8198
.1556
Ti3349
Ppb
497.7
.839
.1686
A13082
ppb
Q432.2
9.11
2.108
Cd2265
ppb
508.3
1.252
.2464
K.7664
ppra
5.204
.0272
.5225
Ni2316
ppb
507.5
1.15
.2267
1960-2
ppb
511.1
.6881
.1346
T11908
ppb
513.5
3.944
.7681
AS1890
ppb
518.4
1.35
.2605
Ce4186
Ppb'
504.2
1.592
.3157
U6707
PPb
497.5
4.19
.8423
P.2149
PPb
522.2
6.02
1.153
Pb2203
ppb
503.3
2.774
.5513
V_2924
PPb
515.0
1.022
.1985
B.2496
ppb
4301.
431.4 .
10.03
C02286
ppb
516.5
1.185
.2294
Hg2790
ppb
506.2
5.785
1.143
2203-1
ppb
508.0
5.345
1.052
Sel960
ppb
516.4
.2838
.055
Zn2062
ppb
514.6
3.424
.6655
8a4934
ppb
509.3
1.147
.2252
Cr2677
ppb
511.4
1.083
.2117
Nn2576
ppb
509.9
1.03
.202
2203-2
ppb
500.9
6.825
1.363
Snl899
ppb
506.0
.7443
.1471
Si2881
PPb
044760.
1116
2.493
Be3130
PPb
526.6
1.61
.3057
CU3247
ppb
502.9
2.779
.5526
M02020
ppb
508.2
2.182
.4294
Sb2068
ppb
494.3
5.041
1.02
Sr4215
ppb
502.4
.6572
.1308
-------
~> Analysis Report Averages
Ned 10-08-97 07:03:45 AH page 45
Method: TRIANGL2 Sasple Nans: ICB/CC8 Operator: DXH
Run Tine: 10/08/97 06:50 Filename: 100797
Node: CONC Type: Q Corr. Factor: 1.00000
Lab ID.: Oust. Snpl. ID.: Cust. ID.: 43231
Elems
Units
Avge
SOev
*RSD
Elents
Units
Avge
SDev
%RSD
Elems
Units
Avge
SDev
$RSD
Elems
Units
Avge
SDev
%RSD
Elems
Units
Avge
SDev
IRSD
Elems
Units
Avge
SDev
WSD
Ag3280
ppb
.1747
.2575
147.4
Ca3179
ppb
1.500
.9785
65.23
Fe2714
PPb
-1.281
6.35
495.6
Na3302
ppm
.0537
.1344
250.4
1960-1
ppb
5.207
2.845
54.64
Ti3349
PPb
-.0724
.1862
257.3
A13082
ppb
Q-74.49
6.276
8.426
Cd2265
ppb
-.2270
.2033
89.54
K.7664
ppn
.0347
.0401
115.5
Ni2316
ppb
.9256
.476
51.42
1960-2
ppb
-3.632
.2124
5.847
T11908
ppb
-1.171
1.804
154
AS1890
ppb
3.113
2.751
88.39
Ce4186
ppb'
-.2441
1.225
501.8
Li6707
ppb
.0343
.0697
203.3
P.2149
PPb
.6120
5.274
861.8
Pb2203
ppb
-1.706
.8566
50.21
V.2924
ppb
-.6510
.6563
100.8
8.2496
ppb
2950.
355.5
12.05
C02286
ppb
-.3791
.6709
177
Ng2790
ppb
-4.398
4.759
108.2
2203-1
ppb
-2.038
3.557
174.5
Sel960
ppb
-.6889
1.058
153.6
Zn2062
ppb
-.8326
.4831
58.02
8a4934
ppb
-.0343
.0694
202.6
Cr2677
ppb
.7813
.8068
103.3
Hn2576
ppb
-.0473
.0454
95.89
2203-2
ppb
-1.540
.5084
33.01
Snl899
ppb
-1.529
2.38
155.6
512881
ppb
Q21830.
2473
11.33
8e3130
ppb
Q-1.163
.0684
5.885
CU3247
ppb
.1096
.0587
53.58
PI02020
ppb
-.4506
.2341
51.95
Sb2068
ppb
.8408
3.233
384.6
Sr4215
ppb
.0044
.033
742.7
282
-------
* Analysis Report Averages
led 10-08-97 07:03:45 AM page 46
Method: TRIAN6L2 Sample Name: ICSA8 Operator: OKH
Run Tine: 10/08/97 06:56 Filename: 100797
Node: CONC Type: Q Corr. Factor: 1.00000
Lab ID.: Cust. Smpl. ID.: Cust. ID.: 43231
El ems
Units
Avge
SOev
IRSD
El eras
Units
Avge
SOev
*RSD
El ems
Units
Avge
SOev
iRSD
Elems
Units
Avge
SOev
iRSD
Elems
Units
Avge
SDev
*RSD
Elens
Units
Avge
SDev
IRSD
Ag3280
ppb
547.0
2.838
.5189
Ca3179
ppb
449600.
5123
1.14
Fe2714
ppb
176900.
1634
.9233
Na3302
ppm
5.784
.1398
2.417
1960-1
ppb
577.0
7.764
1.346
TJ3349
ppb
494.5
3.804
.7693
A13082
ppb
512400.
3670
.7162
Cd2265
ppb
475.8
4.729
.9937
K.7664
PP«
026.31
.0473
.1799
Ni2316
ppb
461.1
5.119
1.11
1960-2
ppb
537.7
10.31
1.917
T11908
ppb
513.6
10.16
1.978
As 1890
ppb
534.7
6.726
1.258
Ce4186
ppb"
504.4
2.094
.4152
U6707
ppb
643.9
1.593
.2474
P.2149
ppb
542.1
22.66
4.181
Pb2203
ppb
489.5
9.074
1.854
V.2924
ppb
506.1
4.613
.9115
BJ496
ppb
3894.
413.9
10.63
C02286
ppb
485.6
4.986
1.027
Mg2790
ppb
535100.
3859
.7211
2203-1
ppb
517.7
5.393
1.042
Sel960
ppb
550.8
5.076
.9217
Zn2062
ppb
457.1
8.895
1.946
B34934
ppb
519,4
2.639
.508
Cr2677
ppb
485.3
6.809
1.403
Mn2576
PPb
466.0
4.417
.948
2203-2
ppb
475.4
14.69
3.09
Snl899
PPb
524. 2
6.615
1.262
Si2881
ppb
Q17280.
2659
15.39
Be3130
PPb
513.4
5.181
1.009
Cu3247
PPb
544.4
3.367
.6184
M02020
PPb
504.6
4.097
.812
Sb2068
PPb
542.9
8.218
1.514
Sr4215
ppb
513.3
2.351
.555
233
-------
AiitoS*i&nler Rfinnrt Table: HA466
Thi! 10-??-0? 01:?«:38 PI*
naa?
Table Naeie: HA466 Autosamoler Type: TYPE TJA
Sanmle Positions: 161/112 QC Positions: 13/1° I Sets: 4
Rinse Station location is rack -I. DOS. -I.
— Rack? —
Rack 9 Type
Usage
1 Aux. Ill Rack STO/GC /BLANK
2 Samole
3 Sanple
4 Samole
5 Samole
I16mra) Sanmles
(16nn) Sanples
(16nn) Samoles
116mm) Sanples
itPos Left Analyses/Pos
13 10
17 1
48 I
48 1
48 1
— Safflole Sat,* —
5et.lt Type
i normal
? Nnr«Ml
A iinrnal
•I Nnrna 1
— Prijoarario
SptJ l.lntake
Preoare? Oescriotion
Ho i.\478
Hn i.W
Ho ».J53o
. II" 4J?.\I
n info — -
UntakeH? Final Oil. Fa
Method KPos Rack* StartPos
TRIAH6L2 II
TRTfttWI." \
[RIAHiiL2 11
TPTAHGL2 (>
rtor
? 1
? !?
2 15
•? 96
No Saraole1: Preoareil
Rack HI
Pos Row Col
1 I
2 1 2
3 1 5
4 1 4
"5 1 5
* 1 A
17.. !9 Hot
Rart- If?
?ns finn i:ol
! 1
•? 1 9
.> I <
4 1 4
5 I 5
f, 1 6
7 I 7
8 ) 8
o I <)
10 1 10
11 1 11
12 1 12
SaiDole Nane Set t
STD3 -NA-
ST01-BLAHIf -HA-
ICSA8 -HA-
CHFCK 1.0 -HA-
iCV/CCV -NA-
ICR/^CB -HA-
Used i
Saniole rtane Set II
1.5478 rtB
d.^47fl LOR
1S5-5?-!
185-57-1 D
185-52-2
185-52-2 HS
185-52-2 HSO
185-52-2 PDS
185-52-2 L
185-52-3
185-52-4
CHECK 997? 2
DUsed Type
? Standard
1 Standard
3 QC Standard
1 QC Standard
5 QC Standard
5 or Standard
HUsed Type
-NA- Saeols
-HA- SauDle
-MA- Sanole
-HA- Saiole
-HA- SanoTe
-NA- Saaole
-NA- Sanole
-NA- Saiole
-NA- Saiole
-NA- Sanple
-NA- Saiple
-NA- Sasole
1-65-^
I-IP^'M
i-^a-tp
234
-------
f <•'
• AutoSamler Reoort Table: HA4fei>
Rack 8°
Pos ROM Col Sanole Nane
Thu 10-23-97 01:29-58 PH
oane 2
Set 8 ((Used
Type
rj
14
15
16
17
18
19
20
21
22
23
24
25
26 •
27
28
?9
JO
';\
W.
Park
vn.
2
2
i
1
I
2
2
2
2
2
2
2
3
3
3
3
5
,\
5
4fi
I*
Kfl.
I
•)
3
4
5
6
7
8
9
10
11
12
1
2
5
4
5
A
7
Nnt
rol
187-68-1
187-68-1 f
4353b MB
43536 ICS
186-11-1
186-11-1 D
186-11-2
186-11-2 MS
186-11-2 MSO
186-11-2 POS .
186-11-2 L
186-11-3
186-11-4
184-23-1A8 XIO
184-23-2A8 XIO
I84-23-2AB XIO POS
184-23-2A8 XIO 1.
IS4-23-3AR VI 0
184-73-5AB XtO OA
iKRd!
SanDle Name
?
n
5
3
5
3
3
3
3
3
3
3
3
4
4
4
4
4
4
Set it
-NA-
-HA-
-Hft-
-HA-
-HA-
-NA- "
-HA-
-HA-
-HA-
-HA-
-HA-
-NA-
-HA-
-NA-
-MA-
-NA-
-HA-
-HA-
-flA-
ttUsed
Satsole
SantDle
Sanole
Sample
Saiole
Saaole
Sample
Sanole
Sample
SaiBDle
Sanole
Sanole
Samole
Samole
Sanole
Samole
Sanole
Saraole
Samole
Tyoe
•I .4ft Nnt IKjP.rli
Rark 84
Pos RON Col Sanols Name
* I...48 Not Used)
Rack «5
Pos RON Col Samole Name
II...48 Mot Used)
Set it KUsed
Tvoe
Set I XUsed
Type
285
-------
Standardization Rot.
Thu 10-25-97 05:12:19 AM paae I
Hethod: TRlftH6L2 Standard: STDI-BIANI1'
f-lein
Avae
SDev
«SP
HI
»?
»S
Flpnt
Avge
SOev
SRSO
11
82
85
El em
Avae
SOev
%RSO
81
«?
85
FlPin
Avae
Sfipv
•5RSO
tt!
«•?
itj.
El era
Avgp
SOev
».RSO
111
82
113
Ag5280
-.0001
.0004
362.7
.0001
.0001
- 0005
Cd?W
-.0003
.0001
38.50
-.0004
-.0002
-.0003
U6707
.1412
.0010
.7015
.1483
.1503
.I486
770.S- 1
0008
.OOOR
lOh.2
001 <•
0009
-.0001
11334"
-.0000
.0005
787.1
-.0003
.0000
.0002
A 1 3082
.002?
.0000
.2999
0025
.0025
.0025
Ce4186
-.0002
.0001
37.20
-.0003
-.0002
-.0002
Mg2790
-.0000
.0001
504.7
- 0002
.0001
.0000
7203-2
-.0001
.000?
J^.S
- . oon?
0001
.0001
T 11908
-.0004
.0001
19.22
-.0005
-.0003
-.0004
As 1890
-.0003
0000
13.71
-.0003
-.0002
-.0003
C02286
- 0002
.0001
44'. 61
-.0003
-.0001
-.0001
Hn2576
.0000
.0000
86.62
0000
.0000
.0000
Sh?06fl
0003
.ooft«;
158 2
- Mm
i)00<)
.000?
VJ994
-J)004
.0000
8.260
-.0005
-.0004
-.0004
6 J496
.0001
.0001
64.94
.0000
.0001
.0002
Cr2677
-.0001
.0001
57.78
-.0002
-.0001
-.0001
Ho2020
.0000
.0001
177.0-
-.0000
0001
0000
I9AO-1
- 0043
.0005
10 55
-.'1047
-.0058
-.0044
Zn?0b2
-.0000
.0001
156.1
-.0001
.0000
-.0000
834934
.0000
.0000
53.64
0000
.0001
.0001
r:»3?47
.0024
.0000
.o536
.0024
.0024
.0024
Na3302
.0027
.0058
142.5
.0048
.0050
- 0017
I960-?
0015
.0006
io.78
. OOIM
00 1 8
.001 °
S12881
.0221
.0004
1.931
.0225
.0221
.0217
8e5130
.0002
.0000
1.422
.0002
.0002
.0002
Fe2714
.0000
.0000
368.2
-.0000
.0000
.0000
N12316
-.0016
.0001
3.309
-.0017
-.0016
-.0016
Snl89o
- 0003
.0001
?<».55
-.000?
-.0004
-.0004
Ca3179
.0006
.0000
4.980
.0005
.0006
.0006
K.7664
7.539
.046
.6274
7.30°
7.392
7.315
P.2149
-"0008
.0001
15.47
-.0007
-.000?
-.0009
Sr4215
.0001
.OOOC'
29.14
.000!
0001
.000!
286
-------
. Standardization Rot. Thu 10-23-97 05:12:19 AH paae ?
IntStd 1 234567
Node *Counts Ti»e NOTUSEO NOTUSED NOTUSED NOTUSED NOTUSED
Eles) y
Wavlen 371.030 -- -- -- -- -- -•
Avge 236811 15000
SOev 5390.643 .OOOOOOC1 -
SRSD ?.276352 .0000000 --
»! 231267 15000
82 237131 15000
tt.s 2470^4 15000
237
-------
i-ation Rot.
Mp.thnd- TRlANfil.? Standard: ST03
Thu 10-23-97 05:17:06 AM
oaae 1
El em
Avge
SDev
IRSD
11
12
15
Elei
ftwge
SOev
iFSO
II
4?
»,'
*•"'.*!«
AVOP
sfifitf
^HSf<
41
»?
»3
Flan
Avge
SDev
ttSD
81
82
»3
flem
Avgp
SOev
»fiSI'
1!
r
43
Ag5280
.4108
.0006
.1362
.4115
.4107
.4103
Cd2265
1.091
.005
.4772
MR*
1.0%
1 09"
1167(17
14. ?S
•>o
1 . .Ufl
14.11
u.y>
14.76
2203-1
.2078
.0005
.2306
.2082
.2080
.2075
T i 3349
!.?Q6
.005
.•7477
1 ?0.i
1 . 9C,R
1 ,'Oh
A 13082
.0177
.0001
.3146
.0177
.0176
.0176
C64186
.1183
.000?
.1608
.MR)
.1183
.1185
«n?7%
. fl W
000?
.7?fto
.0221
.0224
.0223
2203-2
.0183
.0007
.7432
.0975
.0988
.0985
H1908
.0334
0006
1.*5ft
.Wfi
.0.5 '.ft
i>53h
AS 1890
.0520
.0001
.2072
.0521
.0520
.0519
C02286
.1195
.0006
.5024
.1190
1202
.1194
Nn?S7o
.I4AO
0006
.114?
.1462
.1475
.1469
Sb2068
.1215
.0003
.2893
.1214
.1219
.1213
V_?924
.0415
.0001
..si SO
"Ul.i
.041A
.0415
8.2496
.1615
.0009
.5307
.1606
.1619
.1621
Cr2677
.1684
.0008
.4485
.1677
.169?
.1684
Ho2020
.081H
0007
?^q?
.0816
.0820
.0819
l%0-)
.2666
.0010
.3748
.2677
.2665
.2657
in2062
.125?
.0011
.R474
l?40
.1261
.1754
634934
.2846
.0001
.0363
.2848
.2846
.2846
CU3247
.1699
.0004
.2404
.170?
.1694
.W
Na3302
.7056
.004.',
2. "7^
2105
.2042
.2021
1^60-2
1598
.0008
.5188
.158"
.1601
.1604
Si288l
.477h
.0005
.1014
4782
.4774
.4773
8e3130
.2958
.0014
.4699
.2944
.2971
.2960
Fe2714
.0048
.0001
1.065
.0047
.0048
.004fl
Hv?3l6
.3874
.OOlo
.7671
3865
.3885
.3871
Snl899
.1264
.000°
.6798
.1256
.1274
.1263
Ca3l?9
.0277
.0001
.5285
.0276
.0279
.0277
K_7664
24.70
.2?
.8800
24.9?
24.48
24. AO
P. 2 149
.0234
0005
?.03I
.0221
.023"
.0233
Sr4215
.8633
.0008
.0912
.8636
.8640
.8625
288
-------
Standardization Rot. Thu 10-23-°7 05:17:06 AH oaae
FntSM I 2 3 4 5 o 7
Node *Counts Time NOTUSED MOTUSED HOTUSEfi NOTUSEfi MOPISEO
Eleffl r
Wavien 571.030 —
Ovge 242234 iSOOfl
?401.778 .nooonoo --
.0000000 --
«1 244501 15000
«2 239717 15000
«3 242484 15000
239
-------
Analysis Reoori
QC Standard
Method: TRIANGL2 Sasole Name: 3TD5
Run Tine: 10/23/07 05:17:11
Thu 10-23-97 05:21:54 AN page I
Ooerator: SR8
Hode: CONC Corr. Factor: 1
Flera
Dm ts
Svgp.
srmv
tfisn
m
»2
»3
Errors
Value
Range
Elem
Units
Avge
SOev
*RSO
HI
»?
»3
Frrors
•i* I ne
Ranop
Heat
Uni t.c
M'JOP,
Sfmv
*RSn
11
12
13
Errors
Value
Range
Elen
Units
Avge
SOev
IRSO
II
«'•
»S
Frrnr*
Vain?.
Ag3280
DDh
095.1
•?.fl
2810
99fl.'>
092.7
994.5
QC Pass
1000.
5.000
Cd2265
ppb
993.6
3.8
.3851
990.9
qgj.o
998.0
QC. Pass
1000.
S.flflf-
M*>?07
nnh
997 b
Ih. \
1.0.58
986.4
tOlo.
989.Q
QC Pass
1000.
5.000
2203-1
ODD
994. A
8.. 5
.838H
Wl.l
Qflfl.n
1004
NnOHFO.
A13082
DDb
990.4
A. A
6330
907.7
<587.3
986.4
OC Pass
1000.
5.000
Ce4186
ppb
995.1
4.0
.4026
$90.7
0950
998.5
QC. Pas?
1000
s.nno
Mg2790
nnh
097 ?
4.\
.4301
995.0
093.7
1002.
QC Pass
1000.
5.000
2203-2
ppb
996.7
6.7
.6601
096.0
989.9
1003.
MOrHECK
AS 1 890
DDb
998.1
Q
.0942
997.3
997.9
999.2
QC Pass
100ft.
5.000
C02286
DDb
995.4
3.4
.3368
092.7
014.4
090. i
OH P3?<5
1000.
S.OflO
Mn257o
nnh
••W5 . S
2.7
.2704
991.0
993.2
996.3
QC Pass
1000.
5.000
Sb2068
ppb
991.8
5.1
.5156
086.8
00) .s
997 0
or Pass
1000
6.2496
pnb
1005.
5.
.3007
1004.
1002.
1008.
QC Pass
1000.
5.000
Cr2677
ppb
095.0
3.1
.3118
092.8
°93.7
098.0
flO Pas?
1000.
i.noo
Ho20?0
nnh
096.0
4.1
.4162
994.0
004.4
1001.
QC Pass
1000.
5.000
1960-1
ppb
996.6
8.0
.8020
088.1
997.0
1004
NOCHECK
834034
DDb
096.7
1.3
.1341
006.1
098.2
995.7
QC Pass
IQOfl.
5.000
CU3247
ppb
906.6
2.2
.2201
008.8
OOA.h
094.4
QC Pass
1000.
s.ooo
Ha3302
nn»
0 840
.035
.3571
9.881
0.318
9.821
QC Pass
10.00
5.000
1960-2
ppb
996.6
6.6
.6654
1001.
9fl
-------
.Analysis Report
OC Standard
Thu 10-23-97 05:21:54 AM page ?
Range
5.000
5.000
5.000
El era
Units
Avge
SDev
SRSD
Snl899
ppb
995.8
5.1
.3085
Sr4215
ppb
992.1
1.3
.1274
Ti3349
ppb
993.8
2.1
.2103
T11908
PPb
1016.
5.
.4806
V_2924
ppb
995.5
2.3
.2303
Zn2062
ppb
997.6
5.9
.5953
S12881
PPb
9951.
22.
.2193
993.0
995.3
999.1
81
82
83
Frrnrs Of-
value 1000
Ranap S.Ortft
IntSM I
Hnde *0onnt.«
Elera Y
Wavlen 371.030
Avae 241873
990.7
993.2
992.3
QC
1000.
5.000
Trme
15000
994.3
995.5
QC Pas?
1000.
5.000
1010.
1020.
1018.
QC Pass
1000.
5.000
993.0
996.3
997.4
QC Pass
1000.
5.000
994.3
994.0
1004
QC Pass
1000.
5.000
9974.
9930.
9947.
OC Pas?
10000.
1 5 o 7
NDTDSEP HOTUSED HOTDSEO NOTUSEP
SOPV 3779.456 .OOOOnOO --
iRSO 1.562579 .0000000 --
81 239018
82 246159
83 240442
15000
15000
15000
291
-------
Analvsis Recoct
QC Standard
Thu 10-25-97 05:51:26 AM cage 1
Method: TRIANGL2 Sauole Nane: ICV/CCV
Run Tine: 10/23/97 05:26:45
CoiDBP.nt.:
Mode: CflNC Corr. Factor- I
Operator: SRB
Elein
Uni t«
4vqp,
Sfipw
tfisr.
tti
12
IS
F.rrors
Valup
Range
Elfin
Units
Avge
SOev
SRSO
Jl
»9
43
Frrnr*
'In I us
Hangp
Hsu
lim r«
avoB
Sfipw
wso
HI
»2
83
Errors
Value
Range
Eleni
Units
Avge
SOev
iRSn
Jl
IP
«.'.
frrnr*
'/ante
HQ3280
nnh
105.0
•?.o
.3948
498.1
405.5
494.'?
QC Pass
500.0
10.00
Cd2265
ppb
499.8
.0
.1887
408.7
500. \
500.4
Qf Pass
500.0
.0.. V.
1 I.h7fi7
nob
482 S
fl.fi
1.315
472.6
480.1
485.0
QC Pass
500.0
10.00
2203-1
opb
501.5
6.9
1.384
507.3
49.VR
503.3
NnruFr.K
A 15082
nnh
182.6
l.o
.2010
483.3
482.9
481.5
QC Pass
500.0
10.00
Ce4186
ppb
496.2
2.o
.5881
495.2
493.0
490.5
NOCHFfK
H07700
onh
407 1)
4.?
.3448
495.3
493.0
501.8
QC Pass
500.0
10.00
2203-2
ppb
498.4
6.6
1.331
501.6
4°0.7
5u? 7
NOCHFOr
Asl890
r>nb
502.7
1.3
.2618
5fl?.o
501.3
S03.9
QC Pass
500.0
10.00
Co2286
ppb
490.5
1.0
.2033
498.3
500.2
409.9
QC Pass
500.0
10 00
rtn257h
nob
408.4
1.0
.2056
497.2
499.1
408.8
QC Pass
500.0
10.00
Sb2068
ppb
495.3
.7
.1330
495.4
495.8
404. 1
QC Pass
500.0
8.2496
opb
500.3
2.7
.5324
497.3
502.1
501.6
NOCHECK
Cr2677
ppb
499.8
.g
.1836
498.3
500,6
500 0
Qf Pas?
500.0
10.00
M02020
Dr-h
407 6
.7
.1502
496.8
498.3
497. A
QC Pass
500.0
10.00
1960-1
ppb
504.8
4.2
.8374
507.2
400.0
507.3
MOCHFCK
8a4934
ODh
496.0
1.6
.3247
495.3
498.5
496.8
QC Pass
500.0
10.00
Cu3247
ppb
492.6
1.1
.2196
402.4
403.7
491.6
QC Pass
500.')
10.00
Ha3302
DflB
4 700
.20?
4.215
5.020
4.642
4.708
OC Pass
5.000
10.00
1060-2
ppb
497.2
8.1
1.621
503.9
488.3
400.4
NOCHFCK
Be3150
ODD
499.0
_7
.1396
498.3
499.6
499.2
OC Pass
500.0
10.00
Fe2714
ppb
505.2
6.2
1.218
408.1
508.3
508.8
QC Pass
500.0
jo. oo
Ni23l6
noh
501 0
1.8
.3620
500.3
409.7
503.1
OC Pass
500.0
10.00
Pb2203
ppb
400.4
6.6
1.327
503.5
401.7
502.0
OC Pass
500.0
C33179
DDb
490.9
1.0
.1994
498.1
499.8
499.8
QC Pass
500.0
10.00
X.7664
ppn
4.748
.097
2.052
4 636
4.R03
4.306
Qf Pas?
5.000
10.00
P_2140
DBh
400.8
2.8
.5549
407.0
503.0
498.6
QC Pass
500.0
10.00
Sel960
ppb
400.7
6.7
1.348
505.0
492.2
502.0
OC Pas?
500.0
292
-------
Analvsis Reoort
OC Standard
Thu 10-23-97 05:31:26 AH oaoe ?
Range
10.00
10.00
10.00
El en
Units
Avge
SOev
%RSP
HI
82
«3
Firrnr*
Value
fianoP
inr.St.1
Mode
ties
Wav I en
Avge
SOev
SRSO
HI
«2
83
Snl899
ppb
495.4
1.0
.2080
494.2
496. |
495.9
00 Pas«
500.0
10.00
1
*i*ount.s
Y
371.031'
241394
3588.702
1.486655
237275
243844
243064
Sr4215
ppb
494.0
1.4
.2900
492.8
495.6
493.7
Of Pass
500.0
10.00
•>
Tine
--
--
15000
.0000000
.0000000
15000
15000
isoor-
TJ3349
ppb
495.2
l.l
.214
-------
Recoct.
Of; Standard
Thu 10-23-97 05:36:15 AH
oaae 1
Hpthnd: TRIANGI.2 Sannle Nairn: ICR/CCR
Run Time: 10/23/97 05:31:31
Consent:
Mode: CONC Corr. Factor: 1
Operator: SRB
Elen
Unifcr-
Avge
SOev
%RSD
Ag3280
DDD
.9030
.7566
83.78
_8lvW
ppb
2.453
6.365
259.4
As. 1890
ppb
-.0439
1.8488
4212.
f) ?i9h
PDb
8.734
1.929
22.08
RadQ.sJ
ppb
.0301
.0378
125.8
_Je3J.3p_
DDb
-.0055
.0543
987.0
Ca3179
81
02
85
.7556
01.722
.2310
Frrors OC Pass
Vain* .0000
Sange I. 000
9.798
-.9939
-1.444
Of; Pass
.0000
50.00
1.061
-2.178
.9858
Mr.i ts onh
81
8?
85
trrnrs
ftanqp.
Flsin ?9ft.\
Hni r.s opb
L16707
ppb
.2576
.1170
45.41
QC Pass
.onoo
1 . 000
HI
8?
85
Frrors OC Pass OC
Value .0000 .0000
Range 1.000 3.000
Elen
Uni ts
Avge
SOew
SOev
tRSD
tl
82
83
Errors NOCHECX NOCHECK OC Pass NOCHECK NOCHECK OC Pass OC Pass
Value .0000 .0000 .0000
294
-------
Analysis Report.
QC Standard
Thu 10-23-97 05:36:13 AH
page 2
fianoe
i.OOO
2.000
3.000
Flfiffi
Units
AVOP
SOev
SRSD
Sntflii
nob
-.6974
1.5935
228.5
Sr42l5
pt)b
.0328
.0272
83.03
Ti3349
ppb
.ni»4
0802
702.3
T 11908
ppb
010. Ifl
4.15
40.8!
VJ924
ppb
.397?
.1084
27.28
7.n2062
ppb
.2472
.1436
58.0"
812881
ppb
29.00
5.22
18.00
*2
83
.4910
-2.508
-.0751
Errors QC Pass
Value .0000
fianae 13.00
.0586
.0043
.0355
QC Pass
.0000
1.000
.0714
-.0797
.0426
QC Pass
.0000
8.000
014.%
08.120
Q7.456
QC Fail
.0000
5.000
.4412
.2738
.4766
QC Pass
.0000
2.000
.2709
.0933
.3776
IntStd 1 2 3
Mode tfoiints Tine NOTUSEP
El en Y
DUvlen 371.030 -
Avge ?2477<) 1SOOO
SOev ?341.1?a .0000000 --
tRSfi ! 041523 .0000000 —
23.28
30.21
53.50
QC Pass QC Pass
.0000 .0000
12.00 120.0
4567
NOriJSED NOTIJSEO NOTUSED NOTUSEf'
8'
V'
t?
ISOOO
295
-------
Analysis Report QC Standard
Method: TRIAN6L2 Sample Naie: ICB/CCB
Run Tine: 10/23/97 05:37:37
Consent:
Hode: CONC Corr. Factor: I
Thu 10-23-<>7 05:42:19 AH page 1
Operator: SRB
R38
linm
Suns
Sfifiv
•SiRSri
91
»2
13
Errors
Value
Range
El em
Units
Avge
SOev
IRSD
HI
»•>
4.5
Frrnr*.
Ya | MR
Rangp
!-l?n)
'ini rs
*VO«
Sfie»
tRSf)
HI
1?
»3
Errors
Value
Range
E)e»
Uni ts
Avge
SBev
SRSO
HI
!•>
43
trrnrs
7.1 1 ue
Ag3280
pnh
1507
. 43ft.t
?90 . «»
.At^o
0880
-.?5?9
OC Pass
.0000
1. 000
Cd2265
ppb
.1092
.0804
73.60
. 0997
.1930
0340
Qf Pass
.0000
i . nnn
1 ih/07
nnh
A 140
.051*
16.41
.2820
.3735
.286*
OC Pass
.0000
1. 000
2203-1
ppb
.S74S
3.617
A27.S
4 047
- A47J
-•> '7o
MnrHFflK
A 13082
DDD
4.<'14
.fl?4
16.77
4.470
4.399
5.865
OC Pass
.0000
50.00
Ce418h
ppb
^612?
2.516
411.0
-? ?h7
1.7 (A
.? . 39 1
Of Pass
0000
3.000
dfl-.'79i'i
onh
S ortO
5.7?^
102.2
-.9574
8.156
0.401
OC Pass
.0000
30.00
2203-2
ppb
.4M?fl
1.403
?9fl>
-1 02h
.A7<"
l.'Sh
MnfHECK
AS 1890
nnh
1.424
1.09?
76.66
.2400
1.642
2.391
OC Pass
.0000
5.000
C02286
ppb
!4570
.2725
59.63
.1468
.5665
.6577
Of: Pas<
.0000
1.000
rtn?S7h
nnb
.107?
.ftO?7
j.497
.!0°4
.1080
.104?
OC Pass
.0000
2.000
Sb?068
ppb
.8371
1.932
232.'
-.103°
- 4538
3.054
ilC Pass
0000
8.2496
nnb
4.036
.508
12.58
3.465
4.210
4.435
HOCHECK
Cr2677
ppb
.4543
.3563
78.41
.0504
.5fl»o
.7236
QO Pass
.0000
•? . iinn
H02020
nnn
- i)l31
.4898
3739.
.3785
-.5623
.1447
QC Pass
.0000
2.000
1960-1
ppb
-1.029
1.934
188.9
.6933
-.(W
•3.122
NflCHECK
834934
nnn
.1154
.0848
73:41
.0231
.1335
.1897
QC Pass
.0000
•2.000
CU3247
ppb
.3250
.2275
69. °5
.2100
.1781
.5868
Or Pass
.0000
?.iW'
Ha5302
DP»
014?
.144°
1018.
.1534
.0252
-.1358
OC Pass
.0000
300.0
l°-<0-2
ppb
1.980
.620
31.16
1.78"
1 . 403
? o83
HOCHECK
8e3l30
pob
.OOQo
.0103
1189.
.0128
-.0056
-.0045
OC Pass
.0000
1.000
Fe2714
ppb
11.68
5.81
40.75
5.412
16.80
12.75
OC Pass
0000
40. 10
Mi23lo
onh
4814
.8236
171.1
-.1343
.1616
1.4)7
OC Pass
.0000
3.000
Pb2203
ppb
-.5054
.3224
63.79
.8631
.2374
4155
QC Pass
. 0000
Ca3179
DDb
.4210
•J.066
252.7
-.7535
1.326
.6929
OC Pass
.0000
60.00
K.7664
ppn
.1355
.0203
15.01
.1217
.158°
.1259
QC- Pass
OOiiO
??0.''
P.2140
nnh
-1.857
4.051
218.2
-5.068
2.695
-3.197
QC Pass
.0000
30.00
Sel960
ppb
.9838
.3818
38.81
1 424
.7768
. 750?
QC Pass
.0000
296
-------
Analysis Report QC Standard
Thu 10-23-97 05:42:l<» AH
pace ?
Range
4.000
2.000
3.000
El en
Units
Avge
SOev
4HSD
Snl899
ppb
-.6483
1.3390
206.5
SN215
ppb
.0477
.0419
87.76
H3349
ppb
.138?
.1569
1)3.6
T11908
ppb
4.590
2.597
56.58
V_2924
PPb
.5555
.3886
6
3
Hnde *finnnfcs
Hem r
Wavlfin .571.030
Avge 222717
Tin»?
15000
4 S 6 7
NOTUSEf' HOTIISEP NOTIISEP NQTUSEf'
SOflV 3002.896 .OOOOQOfi --
*RSD 1.348303 .0000000 --
»1 220558 15000
82 221446 15000
83 226146 15000
007
-------
Rennrt
Of: Standard
Thu 10-23-07 05:47:05 AM
oaae I
Method: TRIANSI.2 Sanole Na»e: ICSAR
Run lime: 10/23/97 05:42:23
Coninent:
Mode: CONC Corr. Factor: 1
Operator: SRS
Elein
Units
Avge
SOev
IRSO
HI
*2
13
Errors
Vain*
Range
F'iPn
IIPUS
(WOP
^I'lfiV
•JHSn
41
V
»3
Error?
Value
Range
Elen
Uni N
Avge
SflP.V
^PSO
ill
«?
m
>rror<-
'^
nnh
4^.3
1 •>
•-•"ii*,
4^8 1
lfts.°
466.2
QC Pass
500.0
20.00
L16707
DDb
53<>.0
3.?
.6008
54? s
558.5
S.Nf.. 1
unOHErX
?70.\-i
DDb
53*. 8
12.9
2.395
531.6
551.4
527.3
HOCHECK
A 13082
ppb
519600.
5308.
1.022
525600.
517700.
515500.
QC Pass
500000.
20.00
Cpliflh
onb
48P.?
^.i>
. A?S?
•W2.0
486.0
189.4
HOCHECK
Hg2790
pob
546600.
2558.
.4680
S49SOO.
544700.
S45500.
Of: PHSS
SOOono.
?0 00
7703--?
opb
45?."
<».7
2.138
457.4
442. <)
461.3
NflCHECK
AS1890
DDb
518.4
2.0
.3826
519.9
516.2
5I?.2
OC Pass
500.0
20.00
Cn??86
nnh
4M.I
!.?
.'66'
465.4
463.0
465.7
OC Pass
500.0
20.00
Nn2576
pph
451.4
l.«
.4101
4S.M
44<».7
4SI.?
Or Pass
SOO "
20.00
Sh?06R
opb
506.2
3.2
.6304
506.5
502.8
509.1
OC Pass
500.0
B_2496
DDb
516.0
3.1
.6060
518.8
512.6
516.6
NOCHECK
r.rWl
nnb
47^. 1
1.!
.'3.^
478.2
476.0
476. ^
OC Pass
500.0
20.00
1102020
POb
4%. 8
l.«
.3786
498.4
494.8
407.J
QC Pass
snn.o
20.00
I
556.1
556.3
521.6
NOCHECX
8a4934
pob
506.3
3.3
.6436
510.1
504.5
504.4
QC Pass
500.0
20.00
CII324T
opb
508. 9
A.I
!.'S4
51e.l
506. J
504.1
OC Pass
500.0
20.00
Ha3302
PDA
5.02<»
.132
2.610
5.175
4.994
4.9)8
Qf: Pass
5.0
453.4
452.0
455.7
OC Pass
500.0
20.00
Pb2203
pob
481.5
2.2
.4564
482. 1
479.0
483.3
QC Pass
500.0
Ca3l70
DDb
472900.
1345.
.2844
474400.
471700.
472700.
OC Pass
500000.
20.00
K.76M
oora
22. *9
I?
.54^
022.82
22.67
22.58
OC Pass
19.00
20.00
P.2149
onb
482.5
20.5
4.248
481.3
462.7
505.6
QC Pass
500.0
20.00
Sel%0
PPb
521.7
4.7
.8988
525.2
523.6
516.4
OC Pass
500.0
-------
.Analysis Rennet
OC Standard
Thu 10-23-97 05:47:05 AH
pace 2
Sanne
20.00
20.00
20.00
Hen
Units
Avge
SDev
4RSD
81
82
83
Errnrs
Value
Range
IntStd
Mode
Elan
Havien
Avge
SfiPM
*RSO
Snt8°9
oph
49fl. 7
i.o
.7251
502.6
495.5
498.0
QC Pass
500.0
20.00
,
*Cnnnts
Y
571.030
203737
fits. |3Po
. 1000
299
-------
fienort ftveranes Thii 10-25-97 02:50:12 PM oaoe 1
Nfithnd: IRIANGI? Sanole \\w. 184-?5-lAfl V10 Operator:
finn line: 10/23/<>7 13:47 Filenaae: 102317
MnriP: ("OMr IVOR: S Cnrr. Factor: 1.00000
Uh ffJ.: Oust. Siol. ID.: Cust. 10.: 43251
Flems
Units
Avge
SOev
*RSO
fla.wao
nob
12.4
6.018
C02286
ppb
34.15
1.33
3.095
Sel%0
ppb
70.98
1.68
2.367
T 11908
PPb
72.8?
ft. 487
8.909
300
-------
"Analysis Report Averages Thu 10-23-97 02:50:12 PH page 2
Method: TRIANGL2 Sauole Kane: IR4-23-2A8 X10 Operator: SRB
Run Tine: 10/23/97 13:52 Filename: 102397
Node: CONC Tyoe: S Corr. Factor: 1.00000
Lab ID.: Oust. Saol. 10.: Cust. ID.: 43231
FlRBlS
Units opb
AVOP Srt.;.
.387
RfiJl30
opb
IS. 17
.0752
.4954
Co2?8£
oob
42.98
.6077
1.4)4
sumo
ppb
127.4
1.792
1.407
T 11908
ppb
167:7"
5.o
5.34
301
-------
•analysis Report. Averages Thu 10-23-97 02:50:12 PM page 3
Method: TRIAH6L2 Sample Hane: 184-23-2AB X10 POS Operator: SRB
Run Tine: 10/23/97 13:57 FilenaBe: 102397
Mode: CONC Tyoe: S Corr. Factor: 1.00000
Lab ID.: Cust. Snl. ID.: Cust. ID.: 43231
Hems
Units
AVCIR
SDev
*RSn
Ag3280
onb
H7.50
.2254
.?57h
BBS 130
opb
58.87
.1733
.2944
C02286
DDb
9 '
.7723
.884
Sel%0
DDb
175.1
1.258
.7271
Tll"08
PPb
214:?
8.937
4.171
302
-------
Renort Averaaes Thu 10-23-97 02:50:12 PH page 4
Method: TRTANGL? Sanple Nane: 184-23-2AB \10 L Qoerator: SRB
Run Time: 10/23/97 14:02 Filenane: 102397
Node: COHC Tyoe: S Corr. Factor: 1.00000
Lab ID.: Cust. Smol. 10.: Cust. ID.: 43231
El ens
Units
Avge
SDev
%RSD
Ag3280
opb
8.408
.3713
4.416
8e3130
opb
3.464
.0213
.6149
Co2286
ppb
9.450
.1277
1.352
Sel960
ppb
25.07
1.595
6.363
T11908
ppb
35.64'
4.383
12.3
303
-------
Analysis Report. Averages Thu 10-23-97 02-50:12 PM cage 5
Hethnd: TRIAH6L? Sanple Na»fi: 184-23-3AB XIO Operator: SR6
Run Tine: 10/23/97 14:08 Filename: 102397
Hod*: r.m? Tyoe: S Corr. Factor: 1.00000
Ub ID.: Cust. Snol. ID.: Oust. 10.: 43231
Elfli*
Uni ts
Avge
SDev
IRSD
Aq3280
opb
18.90
.4456
2.358
BR3130
ppb
9.108
.0112
.1231
Co2286
ppb
47.27
.4996
1.057
SeWO
ppb
115.6
2.65
2.293
TIJ908
ppb
130!*
7.523
5.740
304
-------
Analysis Reoort Averages Thu 10-23-97 02:50:12 PM page 6
Method: TRIANGL2 Sanole Name: 184-73-3AB X10 DA Ooerator: SR8
Run Time: 10/23/97 14:13 Filenane: 102397
Mode: CflNf: Tvoe: S Corr. Factor: 1.00000
Lab (0.: Cust. Saol. 10.: Cust. ID.: 43231
F.lP.me Ao3?80 Rp.3130 Co??8* Sel9fiO 111908
Units nnh ooh pnb opb ppb
HVOP Ifl.flB 9.051 47.70 llfi.l 139.?
.0407 (,765 I 19| 4.259
.4494 1.418 I.07S 3.0*
305
-------
analysis Reoort Averages
Thu 10-25-<»7 02:50:12 PH
page 7
Method: TRIANGL2 SaiiDle Nane: ICV/CCV Operator: SRB
Run Tine: 10/23/97 14:18 Filenane: 102397
Node: CONC Type: 0 Corr. Factor: 1.00000
Lab ID.: Cust. Snpl. ID.: Cust. ID.: 43231
Flea?
units
AVQR
SDev
iRRf>
Kleins
Mni r.«
AVOP,
Shpw
•5 HSU
FlBUS
Units
AVQP.
SDev
tRSO
El ens
Units
Avge
Sfiev
liRSD
FlPB?
iini r.s
fivgp
Sfiev
tRSft
KlP.ms
Hin N
AVOP.
Sfipy
*Rsn
Ag3280
ppb
503.1
3.32
.66
C3.il 79
nnh
uSbO «
^07 . 4
/» . A
Ffi?7U
ORh
OW.O
804.5
80.6"
Ma3302
pom
4.965
.51
10.27
1960-1
opb
SO,v-3
l?.o.i
•'..^87
m$49
nph
Sui I
h.ll13
1 . >78
A13082
ppb
0567.9
65.94
11. At
01226S
nnh
511.0
A 097
1.1*2
K.7664
opi
4.548
.1051
2.311
Mi2316
npb
510.1
3.816
.748
I960-?
opb
514.7
o 312
l.80«
FIIQ08
nnh
500 ^
a. a??
1.76?
As 1 8<>0
ppb
512.8
6.248
1.218
Ce4-186
PDb
507.0
a. tsi
l.oOS
116707
ppb
469.7
5.841
.8179
P.2149
PDb
0573.7
104.9
18.29
Pb2?03
DDb
0^77.0
50.74
3.794
V_29?4
pnb
505.. \
I..U8
?0o8
R_2496
ppb
610.5
12.97
?. l?5
Co228h
nnh
505.5
•>.4H
. 4905
Ha'^^O
ppb
0937.5
737.1
78.6?
2203-1
pnb
665.6
143.6
21.57
SeH60
nob
511. 1
10.12
1.070
;n?062
nnb
01247.
l?54
100.5
Ba4934
ppb
502 '.\
1.408
.2805
Cr26/7
pob
510.2
4.R24
.9456
Mn2576
DDb
064v. 3
260.3
41.47
2203-2
DDb
532.7
9.081
1.705
Snl8°o
opb
405.:?
23.44
4.734
Si 2881
nnh
139148.
l?fl.n
4.o85
8e3130
ppb
506.o
1.346
.2655
r:n3247
onb
506.6
A.???
1.228
Ho20?0
ppb
504.6
.:,.017
.7763
Sb2068
Dnb
505.4
4.52
.8942
SM?!*
DDb
500.1)
1.306
.2613
-------
s Repnrr.
Thti 10-73-97 0?:50:12 PM page 8
Method: TRIANGI.2 Saaole Hane: IC8/CCB Operator: SR8
Run Tine: 10/23/97 14:24 Filenane: 102397
Mode: CONC Type: Q Corr. Factor: 1.00000
l.ab ID.: r.ust. Suol. ID.: Cust. ID.: 43231
F.IRIB?
Vni ts
HVQR
SDev
SRSf!
lini I*
MVOP
Slip"
FISH)-?
Units
Avge
iflSD
El ens
Units
Avge
SOev
Units
Auofi
.SOev
Hey/feu..
.9285
.221
23.8
Ca3179
DDb
Q7ft3. I
353.5
174.1
F*r/l4
nnb
UV% 7
179 A
15*. 2
Na.«0?
ODD
.2454
.1572
64.08
1960-1
pob
-1.787
I.7fl8
100 /
nw6
onfi
/.04<>
/4.ft72
/ I53.'x-
-BlOUOi HS-18W-
ppb ppb
Q74.76
40.46
54.11
Cd2265
pob
02.463
5.935
15". 7
i 7fto4
npm
0438
.1)771
1?*.?
Hi?3l*
DDb
1.682
2.293
136.3 y
196/2
DO/
/.326I
/7.63
806.3
TH908
oot>
Q*. 377
?.'>7jU—
*4fM
3.028
2.429
80.22
Oe4186
onb
05.986
4.681
70.19
Hh7fl7
nnh
8018
QA?
H3.I /
p 9 v(«
POO
JB2.65
/'I. 22
167.1
Pb2203
PPb
04.054
.5562
13.72
V_79?4
ppb
1 . 94C
-Ti505
103.5
• u>'r.K/ •
ppb
53.81
10.4
19.33
Co2286
DDb
01.418
803
V.A4
nov?9/
nnb/
fl/b I 5
Aw.\
loo
7203-1
DDb
3.052
3.577
117.2
Sel960
DDb
-.8126
1.75
215.4
7n2062
ppb
JJ44V7 _
747
167.6
DdiHJ^ -
ppb
1.973
3.112
157.8
Cr?677
DDb .
07.44JT
3. y\
m.i
Hn257o
pnb
y93.05
160. n
171 5
2703-?
DDb
1.554
1.201
26.37
Snl899
DDb
9.120
13.6
149.1
S17881
opb
a ma1?
268.6
24.82
1 Boaiw ^
ppb j
.6367 /
.6716 /
105.5 /
\jjR\)( 4 /
/^pb
05.365
o.898
178.6
iio2020
DDb
1 487
1.18
70.35
Sb2068
pob
04.814
1.814
37.68
Sr4215
PPb
01.469
2.377
161.8
•
307
-------
Analvsis fleoort Averaaes
Ihii 10-23-97 02:50:12 PM page 9
Nflt.hod: TRlHNGl.? Sample Name: FCB/CCft Operator: SRfi
Rim rime: 10/23/97 U:37 filename: 102397
Mode: CONr fvoe: 0 Corr. Factor: 1.00000
lab 10.: Cust. Snol. ID.: Cust. ID.: 43231
ElfiBS
Units
Avge
SDev
4RSO
El ems
Units
Avge
SOev
SRSO
Flea?
Units
HVQP
SDev
MSP
f IfiBS
lini r.
rtvgs
SIIRV
~RSfi
FIRM
Hni f.s
Avae
SOev
SRSP
Elens
Units
Avge
SDev
iRSO
Ag3280
ppb
.4389
.9499
216.4
Ca3179
DDb
-4.089
1.061
25.96
Fe27l4
oob
-.4611
* . 30*
1010
Mai.W>
nnni
I4?J
.?/4s
192 A
1960-1
opb
1.782
2.798
15.7
Ti3349
ppb
-.0375
.1032
275.3
A 13082
ppb
43.83
3.268
7.455
Cd2265
pob
.0835
.2364
283
K.7664
opn
-.1330
.0685
51. S
N123I6
pn*>
?9|(i
7474
'56. ft
I960-1?
ppb
-.0562
1.641
2921
111908
pob
1.390
3.249
233.7
ft-51890
ppb
.0183
.2873
1566
C64-186
ppb
-1.043
2.254
216.1
H6707
ppb
-.0438
.1492
305. fl
P >U4
nnb
-1.5HO
I 3? 4
.W.8<
Pb2203
Dpb
.737Q
1.157
156.8
V.2924
PDb
.4379
.381
87
8_"496
ppb
19.21
1.032
5.374
C02286
PDb
-.4362
.2649
60.72
Ha2790
ppb
-.0074
3.584
48610
22W-I
opb
3.347
3.74S
III 9
Set 960
ppb
.551°
1.245
?23.9
Zn2062
DDb
5.658
.3572
6.313
8*49.34
ppb
-.0100
.0866
863.1
Cr2677
onh
.0423
.3302
781.2
Hn2576
DOb
. 1?30
0502
40. R)
??OJ-?
onb
-.5649
A. 503
620
Snl899
ppb
-.2662
.5858
219.3
S12881
DDb
80.77
6.595
8.166
BBS 130
ppb
.23K-
.0245
10.58
CU3247
nob
.1351
.1037
76.73
Ho202f'
opb
. !686
.1867
110.7
Sb20h8
ooh
-1 13
1 .\.\6
II 75
Sr4215
ppb
.0011
.0411
3584
303
-------
Analysis Reoort
Averaaes
Thu 10-23-97 02:50:12 PH page 10
Method: TRIANGL2 Sanple Haae: ICSAB Operator: SR8
Run fine: 10/23/97 14:4? Filename: 102397
Mode: CONC Type: Q Corr. Factor- 1.00000
Ub rn.: Cust. SBDI. ID.: Ciist. ID.: 43231
n?»s
Urn N
Avqfl
Sfmv
-*Hsr>
Flems
Units
Avge
SOev
%RSn
El ems
Units
Avge
SOfiv
«SD
F)p.m<;
Units
HVQP
•SIJ8V
*«-?
nnr>
5.il.7
II s?
I US
III 90S
opb
502.5
16.41
3.266
As 1 890
noh
519.8
6.R81
1.324
C.R41R6
ppb
489.8
3.428
.7
116707
DDb
582.5
33.65
5.777
P_?14" •
opb
49R.A
28.6ft
S.751
Pb??0.3
nnh
4fll..i
•4.4?7
9305
V ?9?4
ppb
489.2
3.043
.6222
R .7496
!>nh
540.5
4.63
.8566
ro2?86
ppb
459.7
4.27
.9289
Mg2790
pnb
545000.
3762
.6902
7203-1
onb
504.0
1. 3.. S3
?.644
Se I ^hO
DDh
528.7
i.M?
.3?38
Zn206?
DDb
423.7
7.391
1.744
B34934
Dpb
509.3
7.651
.5204
Cr2677
opb
473.5
4.85
1.024
Mn2576
PDb
438.1
3.381
.7718
7203-7
DDb
469.3
11.84
7.S19
S'nlS'}'}
nob
474. /
4.471
93 M
Si?R8)
DDb
5650.
23.98
.4244
Be3l30
pob
485.4
4.253
.8763
Cu3247
ppb
519.9
6.066
1.167
H02020
PDb
494.7
2.868
.5797
Sb2068
DDb
505.0
10.08
1.995
Sr4?l5
nob
502.0
1.770
.2445
303
-------
flp.nort f?Dl?: IM470
Fhu 10-30-97 07:lbi47 AH pans I
Nan?: Hfl470 Aytwuoler lyoe: fVPE TJA
Positions- (5S/19? QC Positions: 13/19 » Sat?: 5
?. Station location i? racfc -1. oos. -1.
»Pos Uft AnalV53?/Pof.
I
?
3
4
S
—
SP.t,
1
?•
.)
4
S
...
*tl
Hn >
«.,
1
7
3
4
S
6
17..
Rank
Pn<
1
'/
\
1
S
>.
7
H
<»
10
11
AMU i
Satin IP
.Sanolfi
Sa«m|p.
Saaole
Sannle Set
ivoe
Nonal
Hnrnal
Normal
Noraal
Normal
Mnt.'ke
;unnip.c MTP
RON Col
I
7
4
5
6
.14 Not
V
RON i':n I
1
•i
"\
l
S
f.
7
. 8
Q
10
II
U ftack
IIM»B>
1 16991
(Una)
Il6nil
B ...
Prp.nare?
No
(In
No
No
MO
n Tnfn ---
i.ior..i!fp»-'
Sannls Na
STfi3
Sini-BI.AN
ir:SA8
CHECK LO
ICV/CCV
1CB/CC8
Used)
S.innls Na
t.A-7fl
ifn-:>.^-?6
187-32-1
187-37-1
«.to30 Bfi
*3J3o (.CS
187-fc-l
I87-A-1 0
187-4-2
STO/OC/BLAHK
Saaoles
Saenles
Sannlp-;
Sanoles
Oescrintion
43603
4323!
43*>30
4.^1^
I.U4I
Final I'it f:
se Sst »
.-NA-
> -MA-
-NA-
-NA-
-NA-
-NA-
RP. Set t
1
i
ft x'.'oo 2
B X20" P')S ?
XI 00 1
VI Oft Pfl (
5
3
3
3
3
15 10
> ' 1
*n i
48 1
48 1
Method »Pos R
TRIANi5l.2 4
TRIANSI.? ?
TRIANiil.2 11
fPIANfil.2 1 1
TRlAHftl.? 11
rtor
p)p
-MA- S.iBnl/>
-HA- SPHO'P
-MA- Saoole
-NA- Saaole
-NA- Sasoie
-llfl- Sa»Dle
-HA- Saiole
-NA- Saiole
-NA- Saiole
JckK StartPos
't 1
1 *
2 ?
2 if
2 >
-------
Antn3anplp.r Rennet Table: HA470
Rack 9?
Pns ROD Col Saaols Nane
IO-30-«7 07:IAi47 AH woe ?
II ..«8 Not Used)
Rack »4
Pos ROM i:nl Saaole Nans
iI...48 Not Usedl
Rank I1*
Pns PON cnl SanDle Hans
11.. iJi Hnf Used)
Set. « 8llsp.fi
Tvoe
!•>.
13
14
IS
Ih
|7
IH
I'J
•?o
?l
'>?
73
V«
?5
26
'7
28
29
30
31
32
33
.<«
XK
3ft
•:?
/.h
Xu
Uii
H,r,
««
1 ' 12-
? I
'' ?
? .X
? i
9 *
'' ft
•/ 7
•> 8
? °
? 10
2 II
? 1?
.X 1
3 ?
3 3
3 4
3 S
3 ft
.X ?
.x ft
> 9
A in
1 (i
.-. r/
4 1
• •>
•i •.
IK flnf
I.'.
KOM i':o I
187-ft-2 MS
187-6-2 HSP
(87-ft-? PfiS
If 7 -6-? l.
l87-ft-3
I87-A-4
1XMSR nft
d.^l^H I.CS
tfl^-iJO-l
[fift-Qft., [|
1 86-90-?
1 86-00-7 MS
186-90-? MSI)
1 QJLvOl)— 0 DHQ
1 HO " r"'^
186-90-? 1.
186-90-3
186-90-4
43641 M8
43641 I.US
187-17-1
187-17-1 0
I87-I7-?
I8V-I7-? MS
187-17--' HSf'
I87-I/-7 i/DS
187-1 7--J 1
I8M/-A
IM'-'-17-<
IKRrt.
».nl. Na.fi
3
3
3
3
3
3
4
i
4
4
4
4
4
4
4
4
4
5
S
s
S
<•
S
s
5
5
S
s
Set it
-MA-
-NH-
-MA-
-H«-
-MA-
-Hfl-
-HH-
-HA-
-NA-
-Hfl-
-HA-
-HA-
-IIA-
-HA-
-HA-
-MA-
-HA-
-HH-
-HA-
-Hn-
-M«-
-NH-
-MH-
-N«-
-Htt-
-»H-
-HA-
-iio-
BHseil
Saanlfl
Sannli? •
siapift
Sample
Saw 16
Saanl?
S.imnta
saBinIs
S.mnte
Sanol?
Saiolfl
Sanole
saanle
Saiiolp
Sannle
Saople
Sainle
Sanol"
Sanole
SSBplP
Dannie
Sannlp
sannle
Sa.nnlP
Sannle
S.9.Df>l ?
^Aynl 6
S?nple
1 lyoe
Set I tnsed
Fvne
Set I
fvne
311
-------
Fhii 10-30-97 Ot:36i39
oaoe 1
in (n.
p: STC'3 Operator:
01:08 Filenanp,: 103097
Tvnp' 0 Oorr. Factor: 1.00000
am. -Saol. m : I'nst. ID.: 43603
, FlPine
1 Hni ts
u HWOP
SOfiv
' *Rsn
Flems
; Unit*
^ Avoe
Rfipv
tRsn
( 1 p«<5
Units
< AvoB
V SIlP'J
•sisii
/ •
^ !• 1 'I*!'
i!ni"»
/ ' HV1f>
1 SI'S''
~,lt?.\!
r •
1 Flprne
^ Units
HUOP
' SflP.U
; 4RSO
r Elems
' Uni ts
^ Avqe
, „ SOp.v
; tRSD
Aa3?Rf>
onh
1007.
3.0hS
.3043
033170
ppb
1004.
A. 3°
6363
FP.77U
onh •
Hll.V
HI in
•30) S
l4.VV.lf'
r»ni£
•' -iVM
': •' ,',f.
1 Ml
lOfn-l
oob
IOIV?.
S l/fi
.SIAft
Ti334<»
pob
1000.0
3.144
.3144
AUOR?
nnb
qos.o
11.69
1.174
Cd?265
.ppb
1002.
r.95?
2946
K 1M
nnn
« SAO
.IS-JI
i ic;
N) >".\r.
nrn
|IM'|4
i 30?
r.?HS
IPMI-^
oob
1000.
J3. 7«
4.579
T 1 1908
ppb
1004.
13.71
1.366
Asia1"!
oob
1003.
4.141
.413
Ce4186
Rob
998.7
?.932
.2936
UA70/
onh
9>>3."
lfl.M3
1 m
V 7| 1<*
piih
|(H|8
I/I n 7
1 .<«'.
Pb''?(i3
or.n
1006
'24.54
7.44
V.2924
pob
1003.
?.*<»
.2b81
B_?4«6
opb
1007.
2.629
.-7A1I
C02286
pnh
1004.
3.°
.3885
Ma'W
onh
100'?.
l.W
»7fi«
•<'"'A- 1
nnh
1 IK'S .
3 OSh
iflA?
SPI9AO
oob
IrtOJ.
?8.hft
7.863
Zn2062
pob
1008.
3.83<»
.3807
8a*93H
opb
000 (
3.2R5
.3?fi7
Cr2677
pob
lOOh.
3.83S
.3814
Hn?57A
nnb
100.5
3.40?
.?39?
?3ft3-5
nnh
ions.
5V>--'
3 74S
SntflW
opb
1003.
5.028
.5011
Si2881
oob
10020.
43.08
.4301
8*3130
opb
.1005.
2.562
.2551
Cu3247
nnb
1002.
3.041
.3033
Mn?0?0
nnb
tons.
1.307
.13
Sttfl'lhfi
nnh
<»*"» e.
s ^
.V?'''
<5rd-'1S
oob
000 (i
2.51/
.251°
312
-------
flenort
Aweranes
Thu 10-30-97 06:36i39 AH oaoe 3
HRthod: TRTANfiL? Sa«pl« Haw: ICV/CCV Operator: OKH
Run fiae: 10/30/97 01:20 Filenase: 103097
Mode: MM Typp.: 0 Corr. Factor: 1.00000
Lab II).: P.iist. S«o.l. 10..: ' - Cust. ID.: 4360.3
FlPB? Ao3280 A13082
Units nnb onb pob
«VOP S«v> A 490.A 504
SIIP.U h rtHS 21.44 57?
tCW I ->ll 4 371 1.13
RJ496 8*4934 Be3130
ppb nnh ppb
49*. I 502^0" 498.1
11.12 5.951 8.485
•>.?il 1.18* (.705
". 3 -
f I fin*.
llm r.c
41MB
pnh .pnh
SOti S 495J
I •. « IM.IJH
•"' ns; "> osi
nnh
pnh
II "H
•> •>*,<<
nf)h ppb
498.9 504 3
II A o 1170
•>..v»c. I ftdl
(•' I P»«
Hm I*
opb
A7 78
K •;
OPS
cob onb nob
4H9.8 49? I 498 ?
II 7S 28 43 10.09
?.4 5.77r. -?.0?J
nob
400 A
H.?48
I.A5?
rtwgp,
SOsv
tfiSD
P.2I49 2203-1 2203-2 Sb2068
nnw pph nnb ppb pnh poh
5106 496.6 491.0 4974 4946 495.5
.181' 10.07 16.81 18.8S 18.17 9.837
3.548 2.028 3.423 3.79 3.673 1.985
9.7.W
I9AO-? Ph??fi3 Spi9nfl Snlfl00
onb nnh nnb nnh opb nnb
489 8 18fl A 495.5 tiSa.fi 498.rt 498.A
21.5? I? '/6 13.54 11.1? 8 796 6.816
I.76A 1.3*7
!-'|P.»= ii.s.vJ1' III90H V '/si'
tlni f.«; nnh nnh nph nnh pob
MIMA 4«ft ft 4HJ II 49-V 1 4^..i S016.
SIIBV h..'.«S AA If. (0.J9 I? 9K |I2.1
"Hsi; I ''Mr. r. 85 ?.OH ? n|? 2 ?35
313
I ~\
-------
ftpnnrt
• fhn 10-30-97 0*-.tt;.3o AN paop 4
Nflthnrt: fKIAMHl.'J Sasnle Mane: ICfi/Cf:B
Run Tina: IO/3f>/97 OI.-74 Filp.nJtn*: |ft30°7
Node: i:OHC — Type: 0 Corr. factor:
I ah If..-
OpBMtor: fiKH
1.00000
; llni ts
\- Avgs
Sfmv
L
(1 P.»<*
i Hni r.<5
; BVOP
SlIRV
t I P.B«
Uni r«
)•' I P«C
nni ts
HfilDS
Unit?
llni r.s
Aq3280 A1308? As1890 B_2496 8a4934 8e3t30
npb pnb nph neb nob nnb
-18.88 -.8837 2.295 -.348? J^.0419
3 U
SIIP.V
nnh ono nnh
0-10.79 Q-l.hOfl
IS 07 I.10|
I.W ,'
Pb2203 Se|960 Snl899 Sr42IS
nph / nnh nnb pnh nnb poh
.3069 -I.H4 .1508 -.3396 -.1163
f>. M 7.394 1.409 .5844 1.6.35 .1798
.3 780.1 I2(i.5 129.6 481.5 154 6
144.3 310.4
314
-------
fieonrt Avenges
Thu 10-30-97 Oft:36i39 AM D.W. S
Hprhn 1.038
fip.5130
opb opb
-.1773 -.063?
.0824 .0512
64.71 40.47
C42265 Ceil86 Co2286 Cr2677 Cu3247
pnh pnb nnb nph pph ppb
-.2855 -.0974 -1.576 -5120 -.7432 1488
.9311 7.063 .5358 .6873 .7?34
237.1 130.9 104.7 9?.48 486.1
Flpmc
Hni t*
Awflo
Sfiftv
W*l.
MM*
Mm ' e
,i-»n*
::fis.-
'"*
FIMC
llni ts
AVQP
Sfmv
susr.
fleis
Uni ts
Avge
Sfiev
twso
FP.77U K 7664
nnh nnn
-13.85 .OS9S
Irt 48 JiAhl
'S '" «' A(
MAA.I-- rn.'-lr.
n^fii n^^
-l!-'l • ••'•lul
•••I"1. I !>3»
I«S •' ||0 4
l*JAfl-l |OAl>-9
nnn oph
- . ROflo ? . HO
I.321* .<>549
164.? 30.48
Ti3349 TH908
pnh opb
-I. Oil 2.195
1.209 S.7?
II1*. 6 260.7
1 i6707
nnb
.1030
tW
'* p
P -Mrt
onn
-I'l |M
•i H-)'j
Vft . S''
Ph??03
oob
-.1799
.«»77
.UA 1
V_?<»24
DPb
-.8421
.68?fl
81.08
Ho? "O
nnh
-S 14^
4 53 1
S.1>*
-"»,,A-|
rnh
• W\
••> o»
1 3SOO
SPI960
pob
I.IM
.J934
47.4
Zn2062
onb
-.1878
.26?
143.2
Hn?S7ft
pno
- 068 >
0/J>7
II-? •'
•'•Jft5-'
nnh
- I83/
1 !>?ft
SHfc /
Snl*o«
onb
-.107?
1.19
1165
S1288I
nnb
7.441
17.14
230.3
Ho?ft?0
nnh
.PI0
.9J35
SO?.-.
Sh-.'MhH
nrh
- 3nlo
i 5\3
44| H
Sr4'?l<
opb
-.0775
.045*
59.23
315
-------
Rppnrt
Ihn 10-30-97 06.-36i.39 AH
paae 6
J rtnthiuJ: IRIANKI.2 Sasnle Nasm: ICSAB Ooentor: DKH
L Bun HUP.: 10/30/07 QI:3S Filenaup: 1030°?
Rmj8-_f:ilNi: Ivpp.r 0 Corr. Factor: 1.00000
' I ah n- : foist. SBP.I. IP •. Cust. H>.: 43603
Unit*
IHSIl
RO.V.'HO I
nnh nnh oph
v/» «» M«3nO Mil S
•i ftofi e)'\
HPIDS
Uni r.
, ,, SOfiV
nob
V ?q?4
nnb nnb
489.1 487.S
17 4 J 803
3.A19
nnb nob
4?8.3 1430.
ft.45 6S.38
1.973 1.204
316
-------
« HRonrt flveraoes . Ihu lO-3ft-*»7 iifc:3ij;.39 AN oaqfi
i: rpfntlM? Situnlp Hane: •<*•• Si" I .'.'l'J'.r Oop.r?tor: OKH
ftun (IBP- |u/Ail/<)7 0|:S3 Kilfinaiie: 103097
Mndu- rfiiir Tvw S I'iorr. Facfr: 1.00000
l.iti Hi • rriist Sanl. [fi • i':nst.. 10
A^IW Ra40?4 Rp.3130 Cd2?65 Co2286
iinir.« nnh nnh ppb nob pph opb
AVOP 3 303 12.3? 149.3 L8??ft I«8.T L236
Sfifiw .VM4 1.908 .7 .OOfcft 1.932 .1868
SfiSfl 18 (^ IS do .4918
Flans f:r?A77 Hn257A Ni?3l6 P_2149 Pb2203 S52068
ilni !:fl
017
-------
J Analysis Report. Averages . Ihu 10-30-97 06:36^39 AH cage 10
;' MPthnrt- rRTANr,!.? Sasnlfi Nan?.: 4JT \i I X10Q PftJy^
01:57 Filenaae: I05u<»7
Fvne: S Corr. Factor: _ 1.00000
..in ffi.: fiiist. Sanl. 10.: Ctisr.. in.: 43605
r
L
i "ini r.s
I
L «>'09
Sllfi"
j tHSP
flfiBS
,' Units
1 nvgfl
Sfmw
, *HSO
' F|PII<;
.Units
' AWOP
SOev
tfi^n
HU '. ni»
onh
JS A.\
• tr-S.'
i ai
i':r2i>77
nnh
167.8
4.SM
?.7I8
SRI%0
oph
S.VA*
7(12?
I..XOO
oob
ft) AS
I 8'?'.'
•> 9SS
MnW*
pnh
" 10180
MS. 1
2.01S
TIIOOP
nob
SA.sa
5.54<>
«.R06
OPb
I8R.3
1 *h
879S
Mi?jlh
nnh
?« 82
?.!'!
3
7n?06?
opb
S4IHt».
IS42
?.R4a
nnh' onb
SO..U 233 :ff
•J8.V4 5.004
1 W •'.-!<
P 214** Cb2?0.i
nnb oph
1115. %28.
IA ?s tas.f)
I so? I.SI4
Ri?881
pnh
I.WC
16^
1.???
non
50. 9S
1 . 4V7
?.aoi-
Sb2068
nnb
117.8
l.8<»0
1.612
31S
-------
unajucic. pgnnrr ftverin«s . Thu 10-50-17 Oo:4u^23 flfi oa«ie
Hptho<1- TPIftMftl? SpBrde Haw: fCV/C^V Owrator: OKH
fiiin Tina: 10/30/97 0?:15 FHenMe: 10309?
ilnde-
FlPB«
ilni r.s
HVOP
S()P.'.'
Wh
HW
Mr.' re
rfVflr
SI'S"
•!>S"
FI.M
Units
(IVOP
si»ev
tBSfj
Hens
Units
Avge
Sfip.v
do3?ai? A 13082
nob nnb
5071 491 fi
A 8/h 7.??1
I.35S- 1.17
ra3l7<» Cd2265
nnb nnb
SO).? ' 497 9
A. 904 8.731
1 J77 I 754
tf>l\l K ?AM
onh ooffl
MS S -) 7ft?
14 ? 151
••• /M A is^t
rl.1>..'.H'' WT'Mh
nndi nni
j A > / j«jg 14
Al V> > .
<-. 'i! 1 ln|
I1M-I mo-?
nnn nnb
573.1 497 f,
•,^.3« ?5 41
S.04I 5.I5H
Ii3349 Ill'iOS
pnh nnb
499 i) 480 1
7.089 ?7.58
ft? 1890
nob
500.9
5.001
" . 998S
064186
nnb
511 3
13. A7
?.f)6J
1 1^707
nnb
O.'.*
13 IX
•> 7S|
p '.' 1 J«
npp
JVO 0
1 1SK
•„)<*•>
Pb^HW
nnb
507 . ?
?».47
•i.033
V.2924
onb
503.5
fl.373
B ?496
pob
495.8
9 755
1.968
C02286
pnb
501 8
8.6?°
1 72
HOW
onb
•)00. I
« \r>
1 ft"
•'•'(!.<- 1
nnh
V* *. ('
•-!•) ||J
l •'!>
S«I9AO
onb
50' 9
?l 01
4.l«3
M062
nnb
494.8
9.59
8^-1934
opb
50?. P
5. <»3I
».m
Cr2677
Dnh
504.3
7.903
I.5b7
Nn^
onr.
49ft.1;
S.098
'•*"•
««»<-?
nnr-
Son <>
1-) OS
J 58*
Sn!fl«°
nob
49°. 3
6 85ft
1.373
Si 2881
oob
5126.
56.14
&33I3A
DPb
50?.?
8.052
'- m
C«3247
DPb
508.4
7.08»
1. 314
Nn?0?0
nnp
50.1 4
8. .5*?
I>5S
Sb?ftwi
nnh
195 I
a .yi
1 *22
sV4?ts
nob
SOI."
c.317
!.?*»
5.746 1.663 1.138 1.015
319
-------
flnalv<1s Rennrt
Thll 10-30-97 06:40:23 AN MOB 4
• Mflthmt- IRInNiil?
{ Run HBP- io/JD/97
BO
-------
c Hepnrt
. Ihu 10-30-97 Ot:40;?3 «H pane 5
Mpthnd: fRTANGl? Sa»nl* Ha»p.: ICR/CC* Operator: DKH
Bun fine: IO/30/<»7 02:25 Filename: 103097
Mndfi: CONC Tyne: 0 f.nrr. Factor: 1.00000
l.ab m.! niist. Sunl. 10.: . Cnst. ID.: 43231
f IP1B5
uni ts
AUQP
SIIPV
tHSf'
FlPras
llni te
FlPIDC
Hnir.«
PWOP
•SUAV
•SPSi'
h ls«e
llni r<
AViTS
«l!P"
SHSli
nsl8?0
opb
L_ -.U«i?
5562
.W*..ft
R_2496
DDb
-1 ^H1-
.*>lfi«
47. ^S
Ra-1934
nob
-.»4T1
.162
110 ?
893130
OOb
-.0702
.oTTir-
Ifl.-Jft
' lUK ft.\ n
-I 117 .M48 •».!?>•,
.700? .21ft> ?S.8
7u )h ?'?8.l ?ftV ft
> •
nnb
- 0821'1
.0841
r i
321
-------
ftpnnrf
flURMOI?«
Thii U>-30-°7
:W AN
MOP 6
f" rtBthnrt; l'KiflHhi.-> Sannlfl M.«e: [CR/CCR Operator: OKH
^ Run TIBP- Hi/30/07 07:46 Filename: IOJO<>7
node: i;UMf: Fyne: 0 Corr. Factor: 1.00000
, I ah in : f:n<;t
npto nnh nnh
(III IS
rt14'-'
'Hh' .Mill*.
noh
-«J 14-i - 0/58
i-.l A1. HV \.>.
F I RAC
Units
Miav
SPSft
non
Hi'^lf. P 71
nnn nnb
-l.ftJO -s.
4.V6S
??o.\-1
nnh nnh nnh
-i 4AO I.4S? -.6671
l.b-iX 1.373 1.313
IIS.o 1 19 196.6
. Mm'f.«
Avoe
' SOev
nph nnh
-4 16? 4.324
3 397 I.A?3 7990 I.JfM
ftl h? 37.54 151.4 92.37
Ph?203 Sel960 Snl899 Sr4215
nph pnh ooh nnh
1819 1.498
5664 -.0649
7.304 .052
40ft.8 80.18
llnir.^
AVOP
SIIRV
tBSf!
nph
nnh
V ?<»?.<
nob nnh nnh
-.6813 .06°° -30.67
.3056 .08*8 IH 24
44 85 I?? 5°.4ft
f '
L
322
-------
Ihu 10-30-97 Oh:40^?3 «« oage 7
TPfrtHfil? SPBOlp HPBP- fCSft»_
Kim liiBfi- lfi/31'1/97 ft?- SI FilsiMBR- 103097
Operator: MH
Hmfp- irilll"-
1 >h ill •
FIP.<
Units
flVOP
xrip.u
wsr»
Hems
llni ts
awgfi
SDp.v
tKfUi
HP.'
urn r.s
BVQP
SIIP.V
•KSh
h 1 ?!fl«
I'nir*.
-'..Mr
•••'»•,.
3HSI-
flP,c
units
fl"OP
Sllfitf
MSI.
Flens
llni t«
rtvnp.
Sfmw
JHSU
Fvnp- 0
tnrt . Factor:
i':iKt Sanl (d : P.«?f. 1
A0378A
nnh
541.3
h 03
1 114
Ca3179
nnh
459500
f> 7 33
1.465
FP-»M
nnh
I7h/0ft.
•>.M->
1 A)W
IIV'.'M!'.'
nn*
-. -U-.
S33.:>
4M.77
9.147
Ii3349
nnh
495.4
4.13?
.8341
ft I. 3082
nnh
525200.
1908
.3A33
Cd226S
nnb
464.0
6.098
1 314
1! 7AM
nna
Q?4 88
1 571
A "sin
III -'.Mr.
pph
JV"' .',
' ««•>
1 MA
1 •*<.->
nnh
574.4
?5.44
4.8SI
1 11908
nnb
492.4
14.75
•?.99ft
A0890
nnb
513.8
12.0?
'••"
Ce4186
onh
495.6
10.18
2.053
1 i*707
nnh
581?.?
AV iv
S SHI
V '1 1"
PPh
4SS !i
(J«
••/I /•/
Phwcu
nnb
474.?
3.184
.A7IJ
V_?924
ppb
493.5
4.089
.829
R ?49A 8a4034
onb opt)
518.0 5IS.7
?.7'/9 3.35fc
.5?fe<> .MAO
Cn2286 Cr2677
nob nnh
4A2.0 47f>.4
A I8A 7.IS7
1.339 1.502
«o?790 Mn->S7A
nnh nnh
530100. .i4<»>
ftlsj n olM
I.I. to 1 V'.o
'•'1IA-I '7MA- '
r\n^ nnh
Mm X i'jK 3
•A 'm I'J.J?
r. Oil 1 7Hh
f>plOif,o Snt8OQ
nnh nnb
S?'.3 491.1
?.7?2 lo II
.11 A? 3.3?l
MM Si288l
nob pph
435. A 55(>7.
5.834 A4.I7
1.339 1.153
l.oonoo
[f» : 43231
8P.3130
DDb
'490.7
7.546
1.538
Cu3247
nob
530.7
5.383
I.OU
HnMW
nnh
407.8
A '.'8?
«OJ
?5h->0h8
nnh
197 <•
3A 33
? '.M7
Srl?IS
nnb
soa.»
3.0ft3
.A03
323
-------
ID/Weight File: AB811,IDW
Sample Volume: 100 ml
Loc.
Sample ID
Analyst: RICHARDS
Nominal Weight: 1.0 g
Weight
Dilution
0
1
2
3
4
5
6
7
8
9
10
11
12
13
14
15
16
17
18
19
20
22
23
24
25
26
27
23
29
30
31
32
33
34
35
36
37
38
39
40
41
42
43
44
45
46
47
48
49
50
51
52
53
STD BLK
STDl=0.2ug/L v
STD2=0,5ug/L \
ST03=1.0ug/L N. o ,5^ -7 «\ha
STD4=2.0ug/L S *>-vl° c l
STD5=5.0ug/L /
STD6=10.0ug/L .
TrVrA nun/1 n _.r^ r^ Cj Hi
rr>o tt&.
183-3-10 0X10 ^^^. re-(r*ja t|sop-? i^-
183-3-10 DDX10 '
183-3-1E
183-3^f-lE D ^'^S^ST «c
183-3-2B
183-3-28 D
183-3-20
183-3-2D D
(0(1/97
L
324
-------
Loc. Sample ID Weight Dilution
CA
J*T
55
56"
57
58
59
60
61
62
63
64
65
66
67
68
69
70
71
72
73
74
75
76
77
78
79
80
81
82
83
84
85
86
87
88
8?
90
91
92
93
94
95
96
97
98
99
100
101
102
103
104
105
106
107
108
109
, *7 ^ . r^ 1 & C^ O 1 1. £) / C*™^
CCoZ ^fS»/T"7 "u^-
183-3-2E ^To^^fpT'
183-3-2E D '
183-3-3C
183-3-3C DX5
183-3-3C DDX5
183-3-3C MSX5
183-3-3C MSDX5 ^
1OTTOC . 1 _ Oil*/'? 7
lo-5~o™^r v •<• b &-V)f±\p "I***
183-3-2F D r *
CCV3=6.0ug/L 3-Ot$—
-------
Loc. Sample ID
I 110 183-3-6B
111 183-3-6B D
.' 112 CCV3=6.0ug/L
113 CCB3
" 114 183-3-60
, 115 183-3-60 D
116 183-3-6E
L 117 183-3-6E D
118 183-3-6F
' 119 183-3-6F D
i 120 183-3-78
121 183-3-7B D .
' 122 183-3-7C
I 123 183-3-7C DX5
~ 124 183-3-7C 00X5
- 125 CCV4=6.0ug/L
I 126 CC84
127 183-3-70
, .128 183-3-70 0
129 183-3-7E
130 133-3-7E D
131 183-3-7E MS
' 132 1S3-3-7E MSO
L 133 183-3-7F
134 L83-3-7F 0
• 135 183-3-8B
136 183-3-88 0
137 CCV5=6.0ug/L
138 CC85
139 183-3-8C
; 140 183-3-8C 0X5
141 183-3-8C DDX5
' 142 183-3-80
i 143 183-3-80 D
144 183-3-SE
. 145 183-3-8E D
146 183-3-8F
147 183-3-8F D
148 CCV6-6.0ug/L_
149 CCB6
Weight
Dilution
To lc
326
-------
Element File: HG_.MEL
Element: Hg2
Print Data: Main+Suppl.
Print: Calib. Curve
Remarks:
STANDARDS= 3-018-7
QC= 3-018-8
Analyst: RICHARDS
Peak Storage: None
INSTRUMENT: 5100
Wavelength: 253.7 Peak
Signal Type: AA
Read Time: 30.0
Sample Replicates: 1
Standard Replicates: 1
Technique: MRS Version: 7.01
Slit: 0.7 Low
Signal Measurement: Peak Height (5)
Read Delay: 1.0 BOC Time: 2
FLAME:
Flame Type: Air
Oxidant Flow: 10.0 L/min
Flame Sensor: On
Fuel Flow: 2.0 L/min
CALIBRATION:
Solutions
Calib. Blank
Standard 1
Standard 2
Standard 3
Standard 4
Standard 5
Standard 6
Calibration
Calibration
t c TH
i o 1 U
!STD
!STD
!STD
!3TO
!STD
iSTO
Units:
Type:
ID
D 1 V
BLK
1
2
3
4
5
6
ug/L
Linear
Cone !
0.200J
0.500!
1.000!
2 . 000 !
5.000J
lo.ooo;
Sample Units:
ug/L
QC:
Matrix Check Calculations:
% Difference for Dupls: No
% Recovery for Spike: No
Locations:
Locations:
Cone:
327
-------
Element File: HG_.MEL
Date: 09/30/97
Data File: AB811.DAT
Technique: MHS
Remark 1: STANDARDS= 3-018-7
Remark 2: QC= 3-018-8
Element: Hg2
Time: 09:27
ID/Wt File: AB811.IDW
Calib. Type: Linear
Wavelength: 253.7
Slit: 0.7 L
Lamp Current: 0
Energy: 72
Hg2
ID: STD BLK
Seq. No.: 00003 A/S Pos.: — Date: 09/30/97
Replicate 1
' Peak Area (A-s): 0.002
Blank Corrected Pk Height (A): -0.001
Concentration (ug/L ):. -0.026
; Auto-zero performed.
Time: 09:28
Peak Height (A): -0.001
Hg2 ID: STDl=0.2ug/L
Seq. No.: 00004 A/S Pos.: — Date: 09/30/97
Replicate I
Peak Area (A-s): 0.148
Blank Corrected Pk Height (A): 0.006
Concentration (ug/L ): 0.160
standard'number 1 applied. |'0.200]
Correlation coefficient: 1.00000
Time: 09:29
Peak Height (A): 0.006
Slope: 0.0281
Hg2 ID: STD2=0.5ug/L
Seq. No.: 00005
A/S Pos.: —
Sample abs. is greater than that of the largest standard.
Replicate 1 Time: 09:31
Peak Area (A-s): 0.403 ' Peak Height (A): 0,016
•Blank Corrected Pk Height (A): 0.016
Concentration (ug/L ): 0.579
Standard number 2 applied. [0.500]
Correlation coefficient: 0.99265
Slope: 0.0320
Date: 09/30/9'
Hg2 10: 3T03=1.0ug/L
Seq. No.: 00006
A/S Pos.: —
Sample abs. is greater than that of the largest standard.
Replicate 1 Time: 09:32
Peak Area (A-s): 0.915 Peak Height (A): 0.037
Blank Corrected Pk Height (A): 0.037
Concentration (ug/L ): 1.164
Standard number 3 applied. [1-000]
Correlation coefficient: 0.99169
Slope: 0.0362
Date: 09/30/97
Hg2 ID: STD4=2.0ug/L
Seq. No.: 00007
A/S Pos.: —
Sample abs. is greater than that of the largest standard.
"Replicate 1 . Time: 09:33
Peak Area (A-s): 1.749 Peak Height (A): 0.070
Date: 09/30/9^
328
-------
Blank Corrected Pk Height (A): 0.070
Concentration (ug/L ): 1.941
Standard number 4 applied. [2.000]
Correlation coefficient: 0.99832 Slope: 0.0354
Hg2 ID: STD5=5.0ug/L Seq. No.: 00008 A/S Pos.: — Date: 09/30/97
Sample abs. is greater than that of the largest standard.
Replicate 1 •• Time: 09:35
Peak Area (A-s): 4.656 Peak Height (A): 0.189
Blank Corrected Pk Height (A): 0.189
Concentration (ug/L ): 5.331
Standard number 5 applied. [5.000]
Correlation coefficient: 0.99922 Slope: 0.0373
Hg2 ID: STDfa=10.0ug/L Seq. No.: 00009 A/S Pos.: — Date: 09/30/9^
Sample abs. is greater than that of the largest standard.
Replicate 1 Time: 09:36
Peak Area (A-s): 9.123 Peak Height (A): 0.370
Blank Corrected Pk Height (A): 0.370
Concentration (ug/L ): 9.902
Standard number 6 applied. [10.000]
Correlation coefficient: 0.99982 Slope: 0.0371
329
-------
•Element File: HG_.MEL Element: Hg2
Date: 09/30/97 Time: 09:36
Data File: A8811.DAT ID/Wt File: AB811.IDW
Technique: MHS Calib. Type: Linear
Remark 1: STANDARDS= 3-018-7
Remark 2: QC= 3-018-8
Wavelength: 253.7
Slit: 0.7 L
Lamp Current: 0
Energy: 72
Hi Display Calibration - C:\m_USER\flfl,FILES\ELEHEHT\HG..HEL
0.3701
Linear
Corn. Coef.: 8.99982
Slope; Q.Q371
Concentration
18.
330
-------
Element File: HG..MEL Element: Hg2 Wavelength: 253.7
Date: 09/30/97 Time: 09:38 Slit: 0.7 L
Data File: AB811.DAT ID/Wt File: AB811.IDW Lamp Current: 0
Technique: MHS Calib. Type: Linear Energy: 72
Remark 1: STANDARDS= 3-018-7
Remark 2: QC= 3-018-8
Hg2 ID: ICV=4.0ug/L Seq. No.: 00010 A/S Pos.: — Date: 09/30/97
Replicate 1 Time: 09:39
Peak Area (A-s): 3.815 Peak Height (A): 0.157
Blank Corrected Pk Height (A): 0.157
Concentration (ug/L ):. 4.229
Hg2 ID: ICB Seq. No.: 00011 A/S Pos.: — Date: 09/30/97
Replicate 1 Time: 09:41
Peak Area (A-s): 0.015 Peak Height (A): 0.001
Blank Corrected Pk Height (A): 0.001
Concentration (ug/L ): 0.014
Hg2 ID: CHECK. LO Seq. No.: 00012 A/S Pos.: -- Date: 09/30/97
Replicate 1 Time: 09:42
Peak Area (A-s): 0.194 Peak Height (A): 0.008
Blank Corrected Pk Height (A): 0.008
Concentration (ug/L ): 0.208
Hg2 ID: 43159A MB3 Seq. No.: 00013 A/S Pos.: — Date: 09/30/97
Replicate 1 Time: 09:46
Peak Area (A-s): 0.009 Peak Height (A): 0.001
Blank Corrected Pk Height (A): 0.001
Concentration (ug/L ): 0.014
Hg2 ID: 43159A MB3 D Seq. No.: 00014 A/S Pos.: — Date: 09/30/97
Replicate L Time: 09:47
Peak Area (A-s): 0.018 Peak Height (A): 0.001
Blank Corrected Pk Height (A): 0.001
Concentration (ug/L ): 0.038
Hg2 ID: 43159A LCS3 Seq. No.: 00015 A/S Pos.: — Date: 09/30/9"
Replicate f -*. Time: 09:48
Peak Area (A-s): sTzsT^—~->^_ Peak Height (A): 0.132
Blank Corrected Pk Height (A)
Concentration (ug/L '): 3.574
Hg2 ID: 43159A LCS3
Seq. No.: 00016
Date: 09/30/97
331
-------
Hg2 ID: 182-30-15B D Seq. No.: 00031 A/S Pos.: — Date: 09/30/97
Replicate 1 Time: 10:40
Peak Area ('A-s): 0.017 Peak Height (A): 0.001
31ank Corrected Pk Height (A): 0.001
/oncentration (ug/L ): 0.024
ig2 ID: 182-30-15C Seq. No.: 00032 A/S Pos.: -- Date: 09/30/97
Replicate 1 Time: 10:42
'eak Area (A-s): 0.022 Peak Height (A): 0.001
Jlank Corrected Pk Height (A): 0.001
Concentration (ug/L ):-0.035
~Hg2 ID: 182-30-15C D Seq. No.: 00033 A/S Pos.: -- Date: 09/30/97
leplicate 1 Time: 10:43
r^eak Area (A-s): 0.045 Peak Height (A): 0.002
Blank Corrected Pk Height (A): 0.002
oncentration (.ug/L ): 0.057
'"g2 ID: CCV2=6.0ug/L Seq. No.: 00034 A/S Pos.: — Date: 09/30/9T
"Replicate 1 Time: 10:44
.Peak Area (A-s): 4.570 Peak Height (A): 0.191
lank Corrected Pk Height (A): 0.191
Concentration (ug/L ): 5.150
32 ID: CCB2 Seq. No.: 00035 A/3 Pos.: — Date: 09/30/97
•"splicate 1 Time: 10:45
, =ak Area (A-s): 0.035 Peak Height (A): 0.001
Blank Corrected Pk Height (.A): 0.001
r.oncentration (ug/L ): 0.038
Hg2 ID: 43231 MB1 ' Seq. No.: 00036 A/3 Pos.: — Date: 09/30/97
;plicate 1 Time: 10:46
Peak Area (A-s): 0.028 Peak Height (A): 0.001
"lank Corrected Pk Height (A): 0.001
Micentration (ug/L ): 0.030
I |2 ID: 43231 MB1 D Seq. No.: 00037 A/S Pos.: — Date: 09/30/97
Replicate 1 Time: 10:47
f :ak Area (A-s): 0.025 Peak Height (A): 0.001
L.ank Corrected Pk Height (A): 0.001
Concentration (ug/L ): 0.027
hg2 ID: 43231 LCS1
Seq. No.: 00038 A/S Pos.: — Date: 09/30/97
332
-------
Replicate 1
Peak Area (A-s): 4.465
Blank Corrected Pk Height (A): 0.184
Concentration (ug/L ): 4.979
Time: 10:49
Peak Height (A): 0.184
Hg2 ID: 43231 LCS1 D
Seq. No.: 00039 A/S Pos.: — Date: 09/30/97
Replicate 1
Peak Area (A-s): 4.564
Blank Corrected Pk Height (A): 0.190
Concentration (ug/L ): 5.117
Time: 10:50
Peak Height (A): 0.190
Hg2 ID: 183-3-2C
Seq. No.: 00040 A/S Pos.: — Date: 09/30/97
Replicate 1
Peak Area (A-s): 3.332
Blank Corrected Pk Height (A): 0.140
Concentration (ug/L ): 3.766
Time: 10:51
Peak Height (A): 0.140
Hg2 ID: 183-3-2C D
Seq. No.: 00041
Replicate 1
Peak Area (A-s): 3.501
Blank Corrected Pk Height (A): 0.149
Concentration (ug/L ): 4.031
A/S Pos.: —
Time: 10:52
Peak Height (A): 0.149
Date: 09/30/9:
Hg2 ID: 183-3-2C MS
Seq. No.: 00042 A/S Pos.: — Date: 09/30/97
Replicate 1
Peak Area (A-s): 6.787
Blank Corrected Pk Height (A): 0.283
Concentration (ug/L ): 7.640
Time: 10:53
Peak Height (A): 0.283
Hg2 ID: 183-3-2C MSD
Seq. No.: 00043 A/S Pos.: — Date: 09/30/9:
Replicate 1
Peak Area (A-s): 6.895
Blank Corrected Pk Height (A): 0.292
Concentration (ug/L ): 7.890
Time: 10:54
Peak Height (A): 0.292
Hg2
ID: 183-3-1B
Seq. No.: 00044 A/S Pos.: — Date: 09/30/97
Replicate 1
Peak Area (A-s): 0.076
Blank Corrected Pk Height (A): 0.003
Concentration (ug/L ): 0.087
Time: 10:56
Peak Height (A): 0.003
Hg2 ID: 183-3-1B D
Seq. No.: 00045 A/S Pos.: — Date: 09/30/97
Replicate 1
Peak Area (A-s): 0.072
Blank Corrected Pk Height (A): 0.003
Time: 10:57
Peak Height (A): 0.003
r 1
-------
Concentration (ug/L ): 0.079
Hg2 ID: CCVl=6.0ug/L
Seq. No.: 00046 A/S Pos.: -- Date: 09/30/97
! Replicate 1
Peak Area (A-s): 4.458
Blank Corrected Pk Height (A): 0.188
r Concentration (ug/L ): 5.068
Time: 10:58
Peak Height (A): 0.188
Hg2 ID: CCB1
Seq. No.: 00047
Replicate 1
Peak Area (A-s): 0.050 •
Blank Corrected Pk Height (A): 0.002
Concentration (ug/L ): 0.054
A/S Pos.: --
Time: 10:59
Peak Height (A): 0.002
Date: 09/30/97
Hg2 ID: 183-3-1C
Seq. No.: 00048
A./S Pos.: —
Replicate 1
Peak Area (A-s): 0.039
Blank Corrected Pk Height (A): 0.002
Concentration (ug/L ): 0.043
Time: 11:01
Peak Height (A): 0.002
Date: 09/30/9'
Hg2
ID: 183-3-1C D
Seq. No.: 00049
Replicate 1
Peak Area (A-s): 0.030
Blank Corrected Pk Height (A): 0.002
Concentration (ug/L ): 0.043
A/S Pos.: --
Time: 11:02
Peak Height (A): 0.00^
Date: 09/30/97
Hg2
ID: 183-3-1D
Seq. No.: 00050 A/S Pos.: — Date: 09/30/9:
Sample abs. is greater than that of the largest standard.
Replicate 1 Time: 11:03
Peak Area (A-s): 48.733 Peak Height (A): 1.915
Blank Corrected Pk Height (A): 1.915
Concentration (ug/L ): 51.677
Hg2
ID: 183-3-1D
Replicate 1
Peak Area (A-s): 0.089
Blank Corrected Pk Height
Concentration (ug/L ): 0
0.004
No.: 00051
A/S
Date: 09/30/9'
Time: 11:11
Peak Height (A): 0.004
ID: 183-3-10
Seq. No.: 00052
A/S Pos.: ~
Date: 09/30/9~
Replicate 1
r ''eak Area ( A-
Jlank Corn
ted
0.083
Pk Height (A): 0.003
Time: 11:13
Peak Height (A): 0.003
^"Concentration (ug/L ): 0.087
334
-------
Hg2 ID: 183-3-1E
Seq. No.: 00053 A/S Pos.: — Date: 09/30/9'
Replicate 1
Peak Area (A-s): 0.062
Blank Corrected Pk Height (A): 0.003
Concentration (ug/L ): 0.076
Time: 11:15
Peak Height (A): 0.003
Hg2 ID: 183-3/-1E D
Seq. No.: 00054
Replicate 1
Peak Area (A-s): 0.164
Blank Corrected Pk Height (A): 0.007
Concentration (ug/L ):. 0.176
A/S Pos.: —
Time: 11:17
Peak Height (A): 0.007
Date: 09/30/97
Hd2
ID: 1S3-3-2B
Seq. No.: 00055
Replicate 1
Peak Area (A-s): 0.066
Blank Corrected Pk Height (A): 0.003
Concentration (ug/L ): 0.079
A/S Pos.: —
Time: 11:19
Peak Height (A): 0.003
Date: 09/30/9T
Hg2
ID: 183-3-2B D
Seq. No.: 00056
A/3 Pos.: —
Replicate 1
Peak Area (A-s): 0.078
Blank Corrected Pk Height (A): 0.003
Concentration (ug/L ): 0.087
Time: 11:20
Peak Height (A
0.003
Date: 09/30/9'
ID: 183-3-2D
Seq. No.: 00057
A/S Pos.: —
Replicate 1
Peak Area (A-s): 0.066
Blank Corrected Pk Height (A): 0.003
Concentration (ug/L ): 0.070
Time: 11:21
Peak Height (A): 0.003
Date: 09/30/9^
Hg2 ID: 183-3-2D D
Seq. No.: 00058 A/S Pos.: —
Replicate 1
Peak Area (A-s): 0.068
Blank Corrected Pk Height (A): 0.003
Concentration (ug/L ): 0.073
Time: 11:23
Peak Height (A): 0.003
Date: 09/30/9:
Hg2 ID: CCV2=6.0ug/L
Seq. No.: 00059
Replicate 1
Peak Area (A-s): 4.952
Blank Corrected Pk Height (A): 0.207
Concentration (ug/L ): 5.575
A/S Pos.: —
Time: 11:24
Peak Height (A): 0.207
Date: 09/30/97
Hg2 ID: CCB2
Seq. No.: 00060
A/S Pos.: ™
Date: 09/30/9'
335
-------
Replicate 1
Peak Area (A-s): 0.034
1 lanK Corrected Pk Height (A): 0.001
u oncentration (ug/L .): 0.038
Time: 11:26
Peak Height (A): 0.001
g2
ID: 183-3-2E
Seq. No.: 00061 A/S Pos.: — Date: 09/30/91
fReplicate 1
eak Area (A-s): 0.029
vlank Corrected Pk Height (A): 0.002
Concentration (ug/L ): 0.043
Time: 11:28
Peak Height (A): 0.002
Hg2 ID: 183-3-2E D
L eplicate 1
Peak Area (A-s): 0.432
,Rlank Corrected Pk Height (A): 0.018
oncentration (ug/L ): 0.474
Seq. No.: 00062 A/S Pos.: — Date: 09/30/97
Time: 11:29
Peak Height (A): 0.018
ID: 183-3-3C
Seq. No.: 00063
A/S Pos.: --
Sample abs. is greater than that of the largest standard.
t~eplicate 1 Time: 11:31
1 eak Area (A-s): 20.651 Peak Height (A): 0.866
"Blank Corrected Pk Height (A): 0.866
.Concentration (ug/L ): 23.376
Date: 09/30/9
Hg2
ID: 183-3-3C DX5
Seq. No.: 00064
eplicate 1
Peak Area (A-s): 3.156
•"lank Corrected Pk Height (A): 0.128
oncentration (ug/L ): 3.449
A/S Pos.: —
Time: 11:48
Peak Height (A): 0.128
Date: 09/30/9'
32 ID: 183-3-3C /5DX5 t> Seq. No.: 00065 A/S Pos.: — Date: 09/30/9'
Replicate 1 I0" Time: 11:49
=ak Area (A-s): 3.110 Peak Height (A): 0.127
lank Corrected Pk Height (A): 0.127
Concentration (ug/L ): 3.428
Hg2
ID: 183-3-3C MSX5
Seq. No.: 00066 A/S Pos.: — Date: 09/30/97
! splicate 1
. ^ak Area (A-s): 4.140
Blank Corrected Pk Height (A): 0.168
! sncentration (ug/L ): 4.538
Time: 11:51
Peak Height (A): 0.168
,u-g2 ID: 183-3-3C MSDX5
Replicate 1
Peak Area (A-s): 4.486
Seq. No.: 00067. A/S Pos.: — Date: 09/30/97
Time: 11:53
Peak Height (A): 0.186
336
-------
Blank Corrected Pk Height (A): 0.186
Concentration (ug/L ): 5.011
Hg2 ID: 183-3-2F
Seq. No.: 00068 A/S Pos.: — Date: 09/30/9:
Replicate 1
Peak Area (A-s): 0.781
Blank Corrected Pk Height (A): 0.033
Concentration (ug/L ): 0.891
Time: 11:57
Peak Height (A): 0.033
Hg2
ID: 183-3-2F D
Seq. No.: 00069 A/S Pos.: — Date: 09/30/97
Replicate 1
Peak Area (A-s): 0.424
Blank Corrected Pk Height (A): 0.018
Concentration (ug/L ): 0.479
Time: 11:58
Peak Height (A): 0.018
r l
Hg2 ID: CCV3=6.0ug/L
Seq. No.: 00070 . A/S Pos.: --
Replicate 1
Peak Area (A-s): 5.005
Blank Corrected Pk Height (A): 0.212
Concentration (ug/L ): 5.710
Time: 12:00
Peak Height (A): 0.212
Date: 09/30/9'
Hg2
ID: CCB3
Seq. No.: 00071 A/S Pos.: —
Replicate 1
Peak Area (A-s): 0.040
Blank Corrected Pk Height (A): 0.002
Concentration (ug/L ): 0.049
Time: 12:02
Peak Height (A): 0.002
Date: 09/30/9'
Hg2
ID: 183-3-3B
Seq. No.: 00072 A/S Pos..: —
Replicate 1
Peak Area (A-s): 0.098
Blank Corrected Pk Height (A): 0.004
Concentration (ug/L ): 0.106
Time: 12:04
Peak Height (A): 0.004
Date: 09/30/9^
Hg2
ID: 183-3-3B D
Seq. No.: 00073
Replicate 1
Peak Area (A-s): 0.069
Blank Corrected Pk Height (A): 0.003
Concentration (ug/L ): 0.076
A/S Pos.: —
Time: 12:05
Peak Height (A): 0.003
Date: 09/30/9:
Hg2
ID: 183-3-3D
Seq. No.: 00074 A/S Pos.: —
Replicate 1
Peak Area (A-s): 0.707
Blank Corrected Pk Height (A): 0.030
Concentration .(ug/L ): 0.807
Time: 12:06
Peak Height (A): 0.030
Date: 09/30/97
337
i—i
-------
Hg2 ID: 183-3-30 D
Seq. No.: 00075 A/S Pos.: -- Date: 09/30/97
'u Replicate 1
Peak Area (A-s): 0.715
' Blank Corrected Pk Height (A): 0.029
L Concentration (ug/L ): 0.788
Time: 12:07
Peak Height (A): 0.029
Hg2
ID: 183-3-3E
'Seq. No.: 00076 A/S Pos.: — Date: 09/30/97
Replicate 1
Peak Area (A-s): 0.161
Blank Corrected Pk Height (A): 0.007
Concentration (.ug/L ):-0.187
Time: 12:09
Peak Height (A): 0.007
Hg2 ID: 183-3-3E D
Seq. No.: 00077
A/S Pos.: —
Date: 09/30/9"
Replicate I
Peak Area (A-s): 0.431
.Blank Corrected Pk Height (A): 0.018
Concentration (ug/L ): 0.487
Time: 12:10
Peak Height (A): 0.018
Hg2 ID: 183-3-3F
Seq. No.: 00078 A/S Pos.: -- Date: 09/30/9'
Replicate 1
Peak Area (A-s): 0.169
Blank Corrected Pk Height (A): 0.007
Concentration (ug/L ): 0.181
Time: 12:12
Peak Height (A): 0.007
Hg2 ID: 183-3-3F D
Seq. No..: 00079 A/S Pos.: -- Date: 09/30/97
Replicate i
Peak Area (A-s): 0.351
Blank Corrected Pk Height (A): 0.014
Concentration (ug/L ): 0.387
Time: 12:13
Peak Height (A): 0.014
Hg2 ID: CCV4=6.0ug/L
Seq. No.: 00080 A/S Pos.: — Date: 09/30/97
Replicate 1
Peak Area (A-s): 5.137
Slank Corrected Pk Height (A): 0.216
Concentration (ug/L ): 5.818
Time: 12:14
Peak Height (A): 0.216
ID: CCB4
Seq. No.: 00081 A/S Pos.: —
Replicate 1
3eak Area (A-s): 0.045
-31ank Corrected Pk Height (A): 0.002
Concentration (ug/L ): 0.049
Time: 12:15
Peak Height (A): 0.002
Date: 09/30/97 !
Hg2 ID: 43231 MB2
r ^
I
Seq. No.: 00082 A/3 Pos.: -- Date: 09/30/9-
338
-------
Replicate 1
Peak Area (A-s): 0.032
Blank Corrected Pk Height (A): 0.001
Concentration (ug/L ): 0.035
Time: 13:06
Peak Height (A): 0.001
Hg2 ID: 43231 MB2 D
Seq. No.: 00083 A/S Pos.: — Date: 09/30/9
Replicate 1
Peak Area (A-s): 0.046
Blank Corrected Pk Height (A): 0.002
Concentration (ug/L ): 0.046
Time: 13:07
Peak Height (A;.- 0.002
Hg2 ID: 43231 LCS2
Replicate 1
Peak Area (A-s): 4.566
Blank Corrected Pk Height (A): 0.188
.Concentration (ug/L ): 5.076
Seq. No.: 00084 A/S Pos.: — Date: 09/30/9T
Time: 13:08
Peak Height (A): 0.188
Hg2 ID: 43231 LCS2 D
>vvHntt
Seq . No.: 00085
Replicate 1
Peak Area (A-s): 4.726
Blank Corrected Pk Height (A): 0.196
Concentration (ug/L ): 5.280
A/S Pos.: —
Time: 13:09
Peak Height (A): 0.196
Date: 09/30/9
Hg2
ID: 183-3-4B
Seq. No.: 00086 A/3 Pos.: --
Replicate 1
Peak Area (A-s): 0.053
Blank Corrected Pk Height (A): 0.002
Concentration (ug/L ): 0.060
Time: 13:10
Peak Height (A): 0.002
Date: 09/30/97
Hg2 ID: 183-3-4B D
Seq. No.: 00087 A/S Pos.: -- Date: 09/30/97
Replicate 1
Peak Area (A-s): 0.037
Blank Corrected Pk Height (A): 0.002
Concentration (ug/L ): 0.049
Time: 13:11
Peak Height (A): 0.002
Hg2 ID: 183-3-4C
Seq. No.: 00088
A/S Pos.: --
Replicate 1
Peak Area (A-s): 7.193
Blank Corrected Pk Height (A): 0.293
Concentration (ug/L ): 7.919
Time: 13:12
Peak Height (A): 0.293
Date: 09/30/97
Hg2
ID: 183-3-4C D
Seq. No.: 00089 A/S Pos.: — Date: 09/30/97
Replicate 1
Peak Area (A-s): 7.081
Blank Corrected Pk Height (A): 0.296
Time: 13:14
Peak Height (A): 0.296
-------
L Concentration (ug/L ): 7.987
I. Hg2 ID: 183-3-4C MSX2 Seq. No.: 00090 A/S Pos.: — Date: 09/30/97
I Replicate 1 Time: 13:23
Peak Area (A-s): 4.143 Peak Height (A): 0.174
1 Blank Corrected Pk Height (A): 0.174
Concentration (ug/L ): 4.689
L-
Hg2 ID: 183-3-4C MSDX2 Seq. No.: 00091 A/S Pos.: — Date: 09/30/97
• Replicate 1 Time: 13:24
" Peak Area (A-s): 3.969 . Peak Height (A): 0.162
,• Blank Corrected Pk Height (A): 0.162
Concentration (ug/L ): 4.383
Hg2 ID: CCVl=6.0ug/L Seq. No.: 00092 A/S Pos.: -- Date: 09/30/97
Replicate 1 Time: 13:25
' Peak Area (A-s): 5.289 Peak Height (A): 0.221
, Blank Corrected Pk Height (A): 0.221
Concentration (ug/L ): 5.970
" Hg2 ID: CCB1 Seq. No.: 00093 A/S Pos.: -- Date: 09/30/97
Replicate 1 Time: 13:26
- Peak Area (A-s): 0.061 Peak Height (A): 0.002
Blank Corrected Pk Height (A): 0.002
Concentration (ug/L ): 0.065
\.
' Hg2 ID: 183-3-4D Seq. No.: 00094 A/S Pos.: — Date: 09/30/97
' Replicate 1 Time: 13:30
. Peak Area (A-s): 0.139 Peak Height (A): 0.005
31ank Corrected Pk Height (A): 0.005
Joncentration (ug/L ): 0.143
1g2 ID: 183-3-4D D Seq. No.: 00095 A/S Pos.: -- Date: 09/30/97
' Replicate 1 Time: 13:31
i >eak Area (A-s): 0.128 Peak Height (A): 0.005
vBlank Corrected Pk Height (A): 0.005
Concentration (ug/L ): 0.141
Hg2
ID: 183-3-4E
Seq. No.: 00096 A/S Pos,
Replicate 1
^Peak Area (A-s): 0.668
rRlank Corrected Pk Height (A): 0.027
! :oncentration (ug/L ): 0.726
Time: 13:32
Peak Height (A): 0.027
Date: 09/30/97
340
-------
Hg2 ID: 183-3-4E D
Seq. No.: 00097 A/S Pos.: -- Date: 09/30/97
Replicate 1
Peak Area (A-s): 0.553
Blank Corrected Pk Height (A): 0.022
Concentration (ug/L ): 0.601
Time: 13:33
Peak Height (A): 0.022
Hg2 ID: 183-3-4F
Seq. No.: 00098 A/S Pos.: — Date: 09/30/91
Replicate 1
Peak Area (A-s): 0.093
Blank Corrected Pk Height (A): 0.004
Concentration (ug/L ):. 0.097
Time: 13:34
Peak Height (A): 0.004
r '•
Hg2 ID: 183-3-4F D
Seq. No.: 00099 A/S Pos.: — Date: 09/30/9'
Replicate 1
Peak Area (A-s): 0.121
Blank Corrected Pk Height (A): 0.005
Concentration (ug/L ): 0.125
Time: 13:35
Peak Height (A): 0.005
Hg2 ID: 183-3-5B
Seq. No.: 00100 A/S Pos.:— Date: 09/30/9!
Replicate 1
Peak Area (A-s): 0.034
Blank Corrected Pk Height (A): 0.002
Concentration (ug/L ): 0.043
Time: 13:37
Peak Height (A): 0.002
Hg2 ID: 183-3-5B D
Seq. No.: 00101
A/S Pos.: --
Replicate 1
Peak Area (A-s): 0.042
Blank Corrected Pk Height (A): 0.002
Concentration (ug/L ): 0.054
Time: 13:38
Peak Height (A): 0.002
Date: 09/30/9'
Hg2 ID: 183-3-5C
Seq. No.: 00102 A/3 Pos.: ~ Date: 09/30/97
Replicate 1
Peak Area (A-s): 0.165
Blank Corrected Pk Height (A): 0.007
Concentration (ug/L ): 0.187
Time: 13:39
Peak Height (A): 0.007
Hg2
ID: 183-3-5C D
Seq. No.: 00103 A/S Pos.: — Date: 09/30/9'
Replicate 1
Peak Area (A-s): 0.163
Blank Corrected Pk Height (A): 0.006
Concentration (ug/L ): 0.171
Time: 13:40
Peak Height (A): 0.006
Hg2 ID: CCV2=6.0ug/L
Seq. No.: 00104 A/S Pos.: — Date: 09/30/97
341
-------
Replicate 1
Peak Area (A-s): 5.296
Blank Corrected Pk Height (A): 0.221
Concentration (ug/L ): 5.970
Time: 13:41
Peak Height (A): 0.221
Hg2 ID: CCB2 Seq. No.: 00105 A/S Pos.: — Date: 09/30/97
, Replicate 1 Time: 13:42
: Peak Area (A-s): 0.042 Peak Height (A): 0.002
- Blank Corrected Pk Height (A): 0.002 ~
Concentration (ug/L ): 0.043
Hg2 ID: 183-3-5D - Seq. No.: 00106 A/S Pos.: — Date: 09/30/97
•, Replicate 1 Time: 13:43
'Peak Area (A-s): 0.251 Peak Height (A): 0.010
, Blank Corrected Pk Height (A): 0.010
:oncentration (ug/L ): 0.268
[' \g2 ID: 183-3-5D D Seq. No.: 00107 A/S Pos.: -- Date: 09/30/9'
i
Replicate i Time: 13:45
'-""eak Area (A-s): 0.267 Peak Height (A): 0.011
| Uank Corrected Pk Height (A): 0.011
^Concentration (ug/L ): 0.290
'.,g2 ID: 183-3-5E Seq. No.: 00108 A/S Pos.: — Date: 09/30/97
leplicate 1 rime: 13:46
v 'eak Area (A-s): 0.040 Peak Height (A): 0.002
Blank Corrected Pk Height (A): 0.002 .
• Concentration (ug/L ): 0.043,
,Hg2 ID: 183-3-5E D Seq. No.: 00109 A/S Pos.: — Date: 09/30/97
-.,eplicate 1 Time: 13:47
Peak Area (A-s): 0.050 Peak Height (A): 0.002
' lank Corrected Pk Height (A): 0.002
Dncentration (ug/L ): 0.062
t ~*
', g2 ID: 183-3-6C Seq. No.: 00110 A/S Pos.: — Date: 09/30/97
L
Sample abs. is greater than that of the largest standard. 'imi'"^,«"4-v\ v.
1 splicate 1 Time: 13:48
i,3ak Area (A-s): 36.891 Peak Height (A): 1.483
Blank Corrected Pk Height (A): 1.483
' bncentration (ug/L ): 40.013
f>72 ID: 183-3-6C DX5
Keplicate 1
Peak Area (A-s): 6.469
r1
L
Seq. No.: 00111 A/S Pos.: — Date: 09/30/97
Time: 13:57
Peak Height (A): 0.268
342
-------
Blank Corrected Pk Height (A): 0.268
Concentration (ug/L ): 7.221
Hg2
ID: 183-3-6C
Replicate 1
Peak Area (A-s): 6.584
Blank Corrected Pk Height (A): 0.266
Concentration (ug/L ): 7.183
Seq. No.: 00112 A/S Pos.: — Date: 09/30/97
Time: 13:58
Peak Height (A): 0.266
Hg2
ID: 183-3-6C MSX5
Seq. No.: 00113 A/S Pos.: — Date: 09/30/97
Replicate 1
Peak Area (A-s): 7.506
Blank Corrected Pk Height (A): 0.310
Concentration (ug/L ): 8.355
Time: 14:04
Peak Height (A): 0.310
Hg2 ID: 183-3-6C MSDX5
Seq. No.: 00114 A/S Pos.: -- Date: 09/30/9:
Replicate 1
Peak Area (A-s): 7.662
Blank Corrected Pk Height (A): 0.313
Concentration (ug/L ): 8.436
Time: 14:05
Peak Height (A): 0.313
Hg2 ID: 183-3-6B
Seq. No.: 00115
A/S Pos.: —
Replicate 1
Peak Area (A-s): 0.263
Blank Corrected Pk Height (A): 0.011
Concentration (ug/L ): 0.284
Time: 14:07
Peak Height (A): 0.011
Date: 09/30/9:
Hg2
ID: 183-3-6B D
Seq. No.: 00116 A/S Pos.: -- Date: 09/30/9'
Replicate 1
Peak Area (A-s): 0.070
Blank Corrected Pk Height (A): 0.003
Concentration (ug/L ): 0.076
Time: 14:08
Peak Height (A): 0.003
Hg2 ID: CCV3=6.0ug/L
Seq. No.: 00117 A/S Pos.: -- Date: 09/30/97
Replicate 1
Peak Area (A-s): 5.322
Blank Corrected Pk Height (A): 0.225
Concentration (ug/L ): 6.065
Time: 14:10
Peak Height (A): 0.225
Hg2
ID: CCB3
Seq. No.: 00118 A/S Pos.: --
Replicate 1
Peak Area (A-s): 0.046
Blank Corrected Pk Height (A): 0.002
Concentration (ug/L ): 0.046
Time: 14:11
Peak Height (A): 0.002
Date: 09/30/97
343
-------
(.Hg2 ID: 183-3-6D Seq. No.: 00119 A/S Pos.: — Date: 09/30/97
v Replicate 1 Time: 14:13
Peak Area (A-s): 0.899 Peak Height (A): 0.037
;• Blank Corrected Pk Height (A): 0.037
, Concentration (ug/L ): 1.002
Hg2 ID: 183-3-6D D Seq. No.: 00120 A/S Pos.: — Date: 09/30/97
Replicate 1 ' Time: 14:14
' Peak Area (A-s): 0.895 Peak Height (A): 0.037
1 Blank Corrected Pk Height (A): 0.037
Concentration (ug/L ):. 0.994
{
\
^Hg2 ID: 183-3-6E Seq. No.: 00121 A/S Pos.: — Date: 09/30/97
Replicate 1 Time: 14:15
-Peak Area (A-s): 0.612 Peak Height (A): 0.025
Blank Corrected Pk Height (A): 0.025
I Concentration (ug/L ): 0.666
i
( 'Hg2 ID: 183-3-6E 0 Seq. No.: 00122 A/S Pos.: — Date: 09/30/9~
"""Replicate 1 Time: 14:16
, Peak Area (A-s): 0.634 Peak Height (A): 0.026
; Blank Corrected Pk Height (A): 0.026
concentration (ug/L ): 0.707
^ig2 ID: 133-3-6F Seq. No.: 00123 A/S Pos.: — Date: 09/30/9"
rReplicate 1 Time: 14:17
i 'eak. Area (A-s): 0.822 Peak Height (A): 0.034
"Blank Corrected Pk Height (A): 0.034
Concentration (ug/L ): 0.915
Hg2 ID: 183-3-6F D Seq. No.: 00124 A/S Pos.: — Date: 09/30/97
' .\
, eplicate 1 Time: 14:19
Peak Area (A-s): 0.184 Peak Height (A): 0.008
:"lank Corrected Pk Height (A): 0.008
oncentration (ug/L ): 0.208
f g2 ID: 183-3-76 Seq. No.: 00125 A/S Pos.: — Date: 09/30/97
Replicate 1 Time,- 14:21
[ eak Area (A-s): 0.035 Peak Height (A): 0.002
^Jlank Corrected Pk Height (A): 0.002
Concentration (ug/L ): 0.049
r y
Wg2 ID: 183-3-7B D Seq. No.: 00126 A/S Pos.: — Date: 09/30/9"
r
L
344
-------
Replicate 1
-Peak Area (A-s): 0.105
Blank Corrected Pk Height (A): 0.004
Concentration (ug/L ): 0.114
Time: 14:22
Peak Height (A): 0.004
Hg2 ID: 183-3-7C Seq. No.: 00127 A/S Pos.: — Date: 09/30/97
Sample abs. is greater than that of the largest standard.
Replicate 1 Time: 14:23
Peak Area (A-s): 25.807 ''"Peak Height (A): 1.047
Blank Corrected Pk Height (A): 1.047
Concentration (ug/L ): 28.255
Hg2 ID: 183-3-7C 0X5 Seq. No.: 00128 A/S Pos.: -- Date: 09/30/9
Replicate 1 Time: 14:39
Peak Area (A-s): 4.042 Peak Height (A): 0.167
Blank Corrected Pk Height (A): 0.167
Concentration (ug/L ): 4.508
Hg2 ID: 183-3-7C 1/0X5 D Seq. No.: 00129 A/S Pos.: — Date: 09/30/9
^•n-fWfct
Replicate 1 Time: 14:41
Peak Area (A-s): 4.452 Peak Height (A): O.ISi
Blank Corrected Pk Height (A): 0.181
Concentration (ug/L ): 4.895
Hg2 ID: CCV4=6.0ug/L Seq. No.: 00130 A/S Pos.: -- Date: 09/30/9
Replicate 1 " Time: 14:43
Peak Area (A-s): 5.514 Peak Height (A): 0.235
Blank Corrected Pk Height (A): 0.235
Concentration (ug/L ): 6.354
Hg2 ID: CC84 Seq. No.: 00131 A/S Pos.: -- Date: 09/30/9
Replicate 1 Time: 14:44
Peak Area (A-s): 0.049 Peak Height (A): 0.002
Blank Corrected Pk Height (A): 0.002
Concentration (ug/L ): 0.054
Hg2 ID: 183-3-70 Seq. No.: 00132 A/S Pos.: — Date: 09/30/9
Replicate 1 Time: 14:45
Peak Area (A-s): 1.397 PeaR Height (A): 0.058
Blank Corrected Pk Height (A): 0.058
Concentration (ug/L ): 1.565
Hg2 ID: 183-3-7D D
Replicate 1
Peak Area (A-s): 1.336
Seq. No.: 00133 A/S Pos.: — Date: 09/30/97
Time: 14:46
Peak Height (A): 0.054
-------
L Blank Corrected Pk Height (A): 0.054
Concentration (ug/L ): 1.467
Hg2 ID: 183-3-7E Seq. No.: 00134 A/S Pos.: — Date: 09/30/97
r '
Replicate 1 Time: 14:47
L Peak Area (A-s'): 1.157 Peak Height (A): 0.049
, Blank Corrected Pk Height (A): 0.049
i Concentration (ug/L ): 1.316
i_ "' * .
' Hg2 ID: 183-3-7E D Seq. No.: 00135 A/S Pos.: — Date: 09/30/97
Replicate 1 . Time: 14:49
,- ^eak Area (A-s): 1.133 Peak Height (A): 0.047
, 31ank Corrected Pk Height (A): 0.047
~Concentration (ug/L ): 1.273
- rlg2 ID: 183-3-7E MS Seq. No.: 00136 A/S Pos.: -- Date: 09/30/97
' Replicate 1 Time: 14:50
I >eak Area (A-s): 5.826 Peak Height (A): 0.243
Blank Corrected Pk Height (A): 0.243
•Concentration (ug/L ): 6.555
rHg2 ID: 183-3-7E MSD Seq. No.: 00137 A/S Pos.: — Date: 09/30/97
/
'-replicate 1 Time: 14:51
Peak Area (A-s): 6.085 Peak Height (A): 0.255
f :iank Corrected Pk Height (A): 0.255
.Concentration ('ug/L ): 6.874
r • ' ~ ~~ ~
g2 ID: 183-3-7F Seq. No.: 00133 A/'S Pos.: — Date: 09/30/9'
V,
,Replicate 1 Time: 14:57
eak Area (A-s): 0.092 Peak Height (A): 0.004
^lank Corrected Pk Height (A): 0.004
Concentration (ug/L ): 0.103
; "\
Hg2 ID: 183-3-7F D Seq. No.: 00139 A/S Pos.: — Date: 09/30/97
aplicate 1 Time: 14:58
"Peak Area (A-s): 0.132 Peak Height (A): 0.005
(Blank Corrected Pk Height (A): 0.005
Dncentration (ug/L ): 0.135
"32 ID: 183-3-8B
Seq. No.: 00140 A/S Pos.: — Date: 09/30/9:
Replicate 1
P-?ak Area (A-s): 0.036
! Lank Corrected Pk Height (A): 0.002
concentration (ug/L ): 0.051
f1
L
Time: 14:59
Peak Height (A): 0.002
-------
Hg2 ID: 183-3-88 D
Seq. No.: 00141 A/S Pos.: — Date: 09/30/97
Replicate 1
Peak Area (A-s): 0.032
Blank Corrected Pk Height (A): 0.002
Concentration (ug/L ): 0.043
Time: 15:01
Peak Height (A):
0.002
Hg2 ID: CCV5=6.0ug/L
Seq. No.: 00142 A/S Pos.: -- Date: 09/30/97
Replicate 1
Peak Area (A-s): 5.657.
Blank Corrected Pk Height (A): 0.238
Concentration (ug/L ):. 6.414
Time: 15:02
Peak Height (A): 0.238
Hg2 ID: CCB5
Seq. No.: 00143 A/S Pos.: --
Replicate 1
Peak Area (A-s): 0.034
Blank Corrected Pk Height (A): 0.001
Concentration (ug/L ): 0.032
Time: 15:04
Peak Height (A): 0.001
Date: 09/30/9'
Hg2
ID: 183-3-8C
Seq. No.: 00144 A/S Pos.
Date: 09/30/9
Sample abs. is greater than that of the largest standard.
Replicate 1 Time: 15:06
Peak Area (A-s): 25.797 Peak Height (A): 1.064
Blank Corrected Pk Height (A): 1.064
Concentration (ug/L ): 28.715
Hg2
ID: 183-3-8C DX5
Seq. No.: 00145
A/S Pos,
Date: 09/30/9'
Replicate 1
Peak Area (A-s): 2.095
Blank Corrected Pk Height (A): O.OS6
Concentration (ug/L ): 2.318
Time: 15:15
Peak Height (A): 0.086
Hg2 ID: 183-3-8C 0DX5 C> Seq. No.: 00146 A/S Pos.: — Date: 09/30/9"
Replicate 1 Time: 15:17
Peak Area (A-s): 2.171 Peak Height (A): 0.090
Blank Corrected Pk Height (A): 0.090
Concentration (ug/L ): 2.420
Hg2
ID: 183-3-80
Seq. No.: 00147 ' A/S Pos.: ~
Date: 09/30/9'
Replicate 1
Peak Area (A-s): 0.939
Blank Corrected Pk Height (A): 0.038
Concentration (ug/L ): 1.037
Time: 15:18
Peak Height (A): 0.038
r i
-------
L
, .Hg2 ID: 183-3-8D D
Seq. No.: 00148 A/S Pos.; -- Date: 09/30/9'
Replicate 1
Peak Area (A-s): 0.959
Blank Corrected Pk Height (A): 0.040
Concentration (ug/L ): 1.069
Time: 15:19
Peak Height (A): 0.040
Hg2 ID: 183-3-8E
Seq. No.: 00149 A/S Pos.: — Date: 09/30/97
Replicate 1
Peak Area (A-s): 0.591
Blank Corrected Pk Height (A): 0.024
Concentration (ug/L ):.0.639
Time: 15:21
Peak Height (A): 0.024
Hg2 ID: 183-3-8E D
Seq. No.: 00150
Replicate 1
Peak Area (A-s): 0.568
.Blank Corrected Pk Height (A): 0.023
Concentration (ug/L ): 0.620
A/S Pos.: —
Time: 15:22
Peak Height (A): 0.023
Date: 09/30/9'
Hg2 ID: 183-3-8F
Seq,. No.: 00151
Replicate 1
-Peak Area (A-s): 0.144
Blank Corrected Pk Height (A): 0.006
Concentration (ug/L ): 0.168
A/S Pos.: --
Time: 15:23
Peak Height (A): 0.006
Date: 09/30/9:
Hg2
ID: 183-3-8F 0
Seq. No.: 00152
A/S Pos.: —
' Replicate 1
Peak Area (A-s): 0.082
Blank Corrected Pk Height (A): 0.004
'-Concentration (ug/L ): 0.100
Time: 15:24
Peak Height (A): 0.004
Date: 09/30/97
, Hg2 ID: CCV6=6.0ug/L
Seq. No.: 00153 A/S Pos.: — Date: 09/30/9
^ Sample abs. is greater than that of the largest standard.
Replicate 1 Time: 15:26
' Peak Area (A-s): 25.910 Peak Height (A): 1.066
u 'Blank Corrected Pk Height (A): 1.066
Concentration (ug/L ): 28.780
-Hg2 ID: CCV6=6.0ug/L
Seq. No.: 00154
A/S Pos.: —
1 Replicate 1
--Peak Area (A-s): 8.743
Blank Corrected Pk Height (A): 0.372
['Concentration (ug/L ): 10.047
Time: 15:28
Peak Height (A): 0.372
Date: 09/30/9'
L
348
-------
Hg2 ID: CCB6
Seq. No.: 00155 A/S Pos.: — Date: 09/30/91
Replicate 1
Peak Area (A-s): 0.050
Blank Corrected Pk Height (A): 0.002
Concentration (ug/L ): 0.060
Time: 15:30
Peak Height (A): 0.002
349
r i
-------
ID/Weight File: A6812,IDW
r . Sample Volume: 100 mL
LOG.
Sample ID
Analyst: RICHARDS
Nominal Weight: 1.0 g
-U
Weight
Dilution
\ x o
1 1
2
< 3
1 4
^ 5
6
| 7
I 8
9
10
11
12
r 13
14
" 15
16
r
, 17
!-- 18
19
' ' 20
21
22
r . 23
24
25
26
27
v 28
29
' ' 30
31
( 33
34
35
36
f v
37
38
39
'-' 40
41
^ 42
43
I 44
; 45
46
r 47
L' 48
49
r - 50
51
~ 52
p 53
L
STD BLK
STDl=0.2ug/L >.
STD2=0.5ug/L ^-^ O, - I
STD3=1.0ug/L / "*
ST04=2.0ug/L /
STD5=5.0ug/ /
STD6=10.0ug/L ' ~
ICV-4.0Ug/L — •* ^
ECB
CHECK LO
43159A MB4
43159A MB4 D
43159A LCS4
43159A LCS4 D
182-30-7E
182-30-7E D
182-30-7E MS
182-30-7E MSD
182-30-9E
182-30-9E D -<
CCVl=6.0uq/L -
CCB1
43233B MB
43233B MB D
43233 LCS
43233 LCS D
133-5-1
183-5-1 D
183-5-1 MS
183-5-1 MSD
TCLP BLK.
TCLP BLK D
CCB1
43231 MB3
43231 MB3 D
43231 LCS3
43231 LCS3 D
183-3-1D
183-3-1D D
183-3-2E
183-3-2E D
183-3-2E MS
183-3-2E MSD
(XV1 =6.0ua/L
CCB1 ~~" i~
183-3-2F
183-3-2F D
183-3-3E
183-3-3E D
183-3-3F
183-3-3F D
183-3-1EF
183-3-1EF D
•/'A?
|o/'/V7
350
-------
Loc. Sample ID
54 183-3-5EF
55 183-3-5EF D
56 CCV2=6.0ug/L
57 CCB2
58 183-3-6F
59 183-3-6F D
60 183-3-8C
61 183-3-8C DX2
62 183-3-8C DOX2
63 183-3-8D
64 183-3-8D D
65 183-3-8E
66 183-3-8E 0
67 183-3-8E MS
68 183-3-8E MSO
69 CCV3=6.0ug/L
70 CC83
71 183-3-8F
72 183-3-8F 0
73 CCV4=6.0ug/L
74 CCB4
Weight
Dilution
"/'/V
3-ocy-z.
351
-------
Element File: HG..MEL
.Element: Hg2
Print Data: Main+Suppl.
Print: Calib. Curve
Remarks:
, STANDARDS= 3-019-1
QC= 3-019-2
Analyst: RICHARDS
Peak Storage: None
INSTRUMENT: 5100
Wavelength: 253.7 Peak
Signal Type: AA
Read Time: 30.0
Sample Replicates: 1
Standard Replicates: 1
Technique: MHS Version: 7.01
Slit: 0.7 Low
Signal Measurement: Peak Height (5)
Read Delay: 1.0 BOC Time: 2
' TLAME:
\ Flame Type: Air
* Oxidant Flow: 10.0 L/min
Flame Sensor: On
Fuel Flow: 2.0 L/min
CALIBRATION:
Solutions
Calib. Blank
Standard 1
Standard 2
Standard 3
Standard 4
ID
JSTO BLK
ISTD i
!STD 2
JSTD 3
ISTD 4
Calibration Units: ug/L
Calibration Type: Linear
Cone
0.200!
0.500!
1.000!
2.000!
Sample Units: ug/L
QC:
Matrix Check Calculations:
% Difference for Dupls: No
% Recovery for Spike: No
Locations:
Locations:
Cone:
L
L
352
-------
Element File: HG .MEL Element: Hg2 Wavelength: 253.7
Date: 10/01/97 ~ Time: 09:25 Slit: 0.7 L
Data File: AB812.DAT ID/Wt File: AB812.IDW Lamp Current: 0
Technique: MHS Calib. Type: Linear Energy: 72
Remark 1: STANDARDS= 3-019-1
Remark 2: QC= 3-019-2
Hg2 ID: STD BLK Seq. No.: 00003 A/S Pos.: -- Date: 10/01/97
\ «
Replicate 1 Time: 09:27
Peak Area (A-s): -0.004 Peak Height (A): -0.001
Blank Corrected Pk Height (A): -0.001
Auto-zero performed.
Hg2 ID: STDl=0.2ug/L Seq. No.: 00004 A/S Pos.: — Date: 10/01/9"7
Replicate 1 Time: 09:28
Peak Area (A-s): 0.162 Peak Height (A): 0.007
Blank Corrected Pk Height (A): 0.007
Standard number 1 applied. [0.200]
Correlation coefficient: 1.00000 Slope: 0.0331
Hg2 ID: ST02=0.5ug/L Seq. No.: 00005 A/S Pos.: ~ Date: 10/01/97
Sample abs. is greater than that of the largest standard.
Replicate 1 Time: 09:29
Peak Area (A-s): 0.407 Peak Height (A): 0.017
Blank Corrected Pk Height (A): 0.017
Concentration (ug/L ): 0.503
Standard number 2 applied. [0.500]
Correlation coefficient: 0.99999 Slope: 0.0333
Hg2 ID: STD3=1.0ug/L Seq. No.: 00006 A/S Pos.: — Date: 10/01/97
Sample abs. is greater than that of the largest standard.
Replicate 1 Time: 09:30
Peak Area (A-s): 0.854 Peak Height (A): 0.036
Blank Corrected Pk Height (A): 0.036
Concentration (ug/L ): 1.085
Standard number 3 applied. [1.000]
Correlation coefficient: 0.99780 Slope: 0.0355
Hg2 ID: STD4=2.0ug/L
Seq. No.: 00007 A/S Pos.: ~ Date: 10/01/97
Sample abs. is greater than that of the largest standard.
Replicate 1 Time: 09:32
Peak Area (A-s): 1.759 Peak Height (A): 0.075
Blank Corrected Pk Height (A): 0.075
Concentration (ug/L ): 2.101
-------
bcandard number 4 applied. [2.000]
Correlation coefficient: 0.99899
Slope: 0.0369
Hg2 ID: STD5=5.0ug/
Seq. No.: 00008 A/S Pos.: — Date: 10/01/97
) ample abs. is greater than that of the largest standard.
Replicate 1 Time: 09:33
Peak Area (A-s): 4.364 Peak Height (A): 0.188
! lank Corrected Pk Height (A): 0.188
Concentration (ug/L ): 5.095
tandard number 5 applied. [5.000]
orrelation coefficient: 0.99983
Slope: 0.0375
y; g2 ID: ST06=10.0ug/L
Seq. No.: 00009 A/S Pos.: — Date: 10/01/97
.Sample abs. is greater than that of the largest standard.
1 eplicate 1 Time: 09:34
-. eak Area (A-s): 8.781 Peak Height (A): 0.375
Blank Corrected Pk Height (A): 0.375
oncentration (ug/L ): 10.011
Standard number 6 applied. [LO.OOO]
'Correlation coefficient: 0.99996
Slope: 0.0375
354
-------
Element File: HG_.MEL
Date: 10/01/97
Data File: AB812.DAT
Technique: MHS
Remark 1: STANDARDS= 3-019-1
Remark 2: QC= 3-019-2
Element: Hg2
Time: 09:35
ID/Wt File: AB812.IDW
Calib. Type: Linear
Wavelength: 253.7
Slit: 0.7 L
Lamp Current: 0
Energy: 72
H| Display Calibration - C;\flfl,USER\flflJILES\ELEHEHT\HS,.HEL
0.375n
1.8
Linear
Corn. Coef.: B.99996
Slope; 0.0375
Concentration
1B.B8B
355
-------
.Element File: HG_.MEL Element: Hg2 Wavelength: 253.7
ate: 10/01/97 Time: 09:37 Slit: 0.7 L
-~ata File: AB812.DAT ID/Wt File: AB812.IDW Lamp Current: 0
Technique: MHS Calib. Type: Linear Energy: 72
'^emark 1: STANOARDS= 3-019-1
' amark 2: QC= 3-019-2
. g2 ID: ICV=4.0ug/L Seq. No.: 00010 A/S Pos.: — Date: 10/01/97
.Replicate 1 Time: 09:37
, 'eak Area (A-s): 3.529 Peak Height (A): 0.152
'-lank Corrected Pk Height (A): 0.152
Concentration (ug/L ):- 4.052
\ «,^,«,~^<-^^,«,^.^^~^,«~~^~~~~^.~~«^~^^~~^~^~^^^,~^~~^^^,,
^Hg2 ID: ICB Seq. No.: 00011 A/S Pos.: — Date: 10/01/9~
(eplicate 1 Time: 09:41
'Peak Area (A-s): -0.001 Peak Height (A): 0.000
rBlank Corrected Pk Height (A): 0.000
Concentration (ug/L ): 0.005
( Ig2 ID: CHECK LO Seq. No.: 00012 A/S Pos.: — Date: 10/01/97
Replicate 1 Time: 09:42
r^eak Area (A-s): 0.155 Peak Height (A): 0.006
i Uank Corrected Pk Height (A): 0.006
Concentration (ug/L ): 0.163
( >~~~~.._~~~~~M~~,»~~~~~M~~~~M,>,~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~ra~~~~M~^~~~,.
v.lg2 ID: 43159A MB4 Seq. No.: 00013 A/S Pos.: — Date: 10/01/97
'' teplicate 1 Time: 09:43
u 'eak Area (A-s): -0.001 Peak Height (A): 0.000
' Blank Corrected Pk Height (A): 0.000
- Concentration (ug/L ): 0.003
, Hg2 ID: 43159A MB4 D Seq. No.: 00014 A/S Pos.: -- Date: 10/01/9^
; Replicate 1 Time: 09:44
Peak Area (A-s): -0.004 Peak Height (A): -0.000
I Slank Corrected Pk Height (A): -0.000
; Concentration (ug/L ): -0.005
I Hg2 ID: 43159A LCS4 Seq. No.: 00015 A/S Pos.: — Date: 10/01/97
Replicate 1 Time: 09:45
( =>eak Area (A-s): 3.808 Peak Height (A): 0.164
^~3lank Corrected Pk Height (A): 0.164
Concentration (ug/L ): 4.365
~Hg2 ID: 43159A LCS4 D
Seq. No.: 00016 A/S Pos.: —
r
L
Date: 10/01/97
356
-------
Hg2 ID: 183-5-1 MS
Seq. No.: 00031 A/S Pos.: — Date: 10/01/97
Replicate 1
Peak Area (A-s): 3.985
Blank Corrected Pk Height (A): 0.174
Concentration (ug/L ): 4.632
Time: 10:10
Peak Height (A): 0.174
Hg2 ID: 183-5-1 USD
Seq. No.: 00032 A/S Pos.: — Date: 10/01/97
Replicate 1
Peak Area (A-s): 3.870
Blank Corrected Pk Height (A): 0.166
Concentration (ug/L ):- 4.421
Time: 10:11
Peak Height (A): 0.166
n
Hg2 ID: TCLP BLK
Seq. No.: 00033 A/S Pos.: -- Date: 10/01/97
Replicate 1
Peak Area (A-s): 0.022
Blank Corrected Pk Height (A): 0.001
Concentration (ug/L ): 0.029
Time: 10:12
Peak Height (A): 0.001
Hg2 ID: TCLP BLK D
Seq. No.: 00034 A/S Pos.: — Date: 10/01/97
Replicate I
Peak Area (A-s): 0.046
Blank Corrected Pk Height (A): 0.002
Concentration (ug/L ): 0.051
Time: 10:13
Peak Height (A): 0.002
Hg2 ID: CCVl=6.0ug/L
Seq. No.: 00035 A/S Pos.: -- Date: 10/01/97
Replicate 1
Peak Area (A-s): 5.244
Blank Corrected Pk Height (A): 0.227
Concentration (ug/L ): 6.042
Time: 10:14
Peak Height (A): 0.227
Hg2
ID: CCB1
Seq. No.: 00036 A/S Pos.: -- Date: 10/01/97
Replicate 1
Peak Area (A-s): 0.018
Blank Corrected Pk Height (A): 0.001
Concentration (ug/L ): 0.024
Time: 10:15
Peak Height (A): 0.001
Hg2
ID: 43231 MB3
Seq. No.: 00037 A/S Pos.: — Date: 10/01/97
Replicate 1
Peak Area (A-s): 0.009
Blank Corrected Pk Height (A): 0.000
Concentration (ug/L ): 0.008
Time: 10:16
Peak Height (A): 0.000
Hg2 ID: 43231 MB3 D
Seq. No.: 00038 A/S Pos.: —
Date: 10/01/97
357
-------
t
Replicate 1
, Peak Area (A-s): 0.008
Jlank Corrected Pk Height (A): 0.000
-Concentration (ug/L ): 0.011
Time: 10:17
Peak Height (A): 0.000
L Ig2 ID: 43231 LCS3 Seq. No.: 00039 A/S Pos.: — Date: 10/01/97
' Replicate 1 Time: 10:18
Area (A-s): 3.968 Peak Height (A): 0.174
Corrected Pk Height (A): 0.174"
. Concentration (ug/L ): 4.646
Hg2 ID: 43231 LCS3 D . Seq. No.: 00040 A/S Pos.: — Date: 10/01/97
_ teplicate 1 Time: 10:19
Peak Area (A-s): 3.809 Peak Height (A): 0.165
; Hank Corrected Pk Height (A): 0.165
Concentration (ug/L ): 4.400
r
\g2 ID: 183-3-1D Seq. No.: 00041 A/S Pos.: ~ Date: 10/01/9^
Replicate 1 Time: 10:20
( >eak Area (A-s): 0.031 Peak Height (A): 0.001
;_ 31ank Corrected Pk Height (A): 0.001
Concentration (ug/L ): 0.027
r >•
Hg2 ID: 183-3-1D D Seq. No.: 00042 A/S Pos.: — Date: 10/01/97
teplicate 1 Time: 10:21
^eak Area (A-s): 0.028 Peak Height (A): 0.001
Blank Corrected Pk Height (A): 0.001
Concentration (ug/L ): 0.029
*• ~~~~~~~~-
- Mg2 ID: 183-3-2E Seq. No.: 00043 A/S Pos.: — Date: 10/01/97
s Replicate 1 Time: 10:22
{ Reak Area (A-s): 0.620 Peak Height (A): 0.026
l Hank Corrected Pk Height (A): 0.026
--concentration (ug/L ): 0.698
[_ !g2 ID: 183-3-2E 0 Seq. No.: 00044 A/S Pos.: — Date: 10/01/97
/-Replicate 1 Time: 10:24
( "eak Area (A-s): 0.652 Peak Height (A): 0.027
'Blank Corrected Pk Height (A): 0.027
Concentration (ug/L ): 0.730
Hg2
ID: 183-3-2E MS
Seq. No.: 00045 A/S Pos.: — Date: 10/01/97
Jeplicate 1
Peak Area (A-s): 4.515
^lank Corrected Pk Height (A): 0.194
Time: 10:25
Peak Height (A): 0.194
358
-------
Concentration (ug/L ): 5.183
Hg2 ID: 183-3-2E USD
Seq. No.: 00046 A/S Pos.: — Date: 10/01/97
Replicate 1
Peak Area (A-s): 4.456
Blank Corrected Pk Height (A): 0.190
Concentration (ug/L ): 5.076
Time: 10:26
Peak Height (A): 0.190
Hg2 ID: CCVl=6.0ug/L
Seq. No.: 00047 A/S Pos.: — Date: 10/01/97
Replicate 1
Peak Area (A-s): 5.079 .
Blank Corrected Pk Height (A): 0.219
Concentration (ug/L ): 5.828
Time: 10:27
Peak Height (A): 0.219
Hg2 ID: CCB1
Seq. No.: 00048 A/S Pos.: — Date: 10/01/9'
Replicate 1
Peak Area (A-s): 0.033
Blank Corrected Pk Height (A): 0.001
Concentration (ug/L ): 0.037
Time: 10:28
Peak Height (A): 0.001
Hg2 ID: 183-3-2F
Seq. No.: 00049
Replicate 1
Peak Area (A-s): 0.065
Blank Corrected Pk Height (A): 0.003
Concentration (ug/L ): 0.067
A/S Pos.: —
Time: 10:29
Peak Height (A): 0.003
Date: 10/01/97
Hg2 ID: 183-3-2F D
Seq. No.: 00050 A/S Pos.: — Date: 10/01/97
Replicate 1
Peak Area (A-s): 0.055
Blank Corrected Pk Height (A): 0.002
Concentration (ug/L ): 0.064
Time: 10:30
Peak Height (A):
0.002
Hg2 ID: 183-3-3E
Seq. No.: 00051 A/S Pos.: — Date: 10/01/97
Replicate 1
Peak Area (A-s): 1.023
Blank Corrected Pk Height (A): 0.044
Concentration (ug/L ): 1.174
Time: 10:31
Peak Height (A): 0.044
Hg2 ID: 183-3-3E D
Replicate 1
Peak Area (A-s): 1.080
Blank Corrected Pk Height (A):
Concentration (ug/L ): 1.217
Seq. No.: 00052 A/S Pos.: -- Date: 10/01/9'
0.046
Time: 10:33
Peak Height (A): 0.046
359
n
-------
.
Hg2
ID: 183-3-3F
Seq. No.: 00053 A/S Pos.: — Date: 10/01/97
Replicate 1
Peak Area (A-s): 0.049
Blank Corrected Pk Height (A): 0.002
Concentration (ug/L ): 0.062
Time: 10:34
Peak Height (A): 0.002
ID: 183-3-3F D
Seq. No.: 00054 A/S Pos.: — Date: 10/01/97
, Replicate 1
• =eak Area (A-s): 0.047
31ank Corrected Pk Height (A): 0.002
Concentration (ug/L ):. 0.053
Time: 10:35
Peak Height (A): 0.002
ID: 183-3-1EF
Seq. No.: 00055
A/S Pos.: —
teplicate 1
"Peak Area (A-s): 0.008
, Blank Corrected Pk Height (A): 0.000
Concentration (ug/L ): 0.008
Time: 10:38
Peak Height (A): 0.000
Date: 10/01/9
ig2
ID: 183-3-1EF D
Seq. No.: 00056
A/S Pos.: --
Replicate 1
r^eak Area (A-s): 0.023
Uank Corrected Pk Height (A): 0.001
""Concentration (ug/L ): 0.024
Time: 10:39
Peak Height (A): 0.001
Date: 10/01/9
,ig2
ID: 183-3-5EF
Seq. No.: 00057 A/S Pos.: — Date: 10/01/97
; teplicate 1
:_ 'eak Area (A-s): 0.012
Blank Corrected Pk Height (A): 0.000
^ Concentration (ug/L ): 0.011
Time: 10:40
Peak Height (A): 0.000
Hg2
ID: 183-3-5EF D
Seq. No.: 00058 A/S Pos.: — Date: 10/01/97
,
-------
Replicate 1
Peak Area (A-s): 0.016
Blank Corrected Pk Height (A): 0.000
Concentration (ug/L ): 0.011
Time: 10:44
Peak Height (A): 0.000
Hg2 ID: 183-3-6F Seq. No.: 00061 A/S Pos.: — Date: 10/01/97
Replicate 1 • Time: 10:46
Peak Area (A-s): 0.023 Peak Height (A): 0.001
Blank Corrected Pk Height (A): 0.001 "
Concentration (ug/L ): 0.027
Hg2 ID: 183-3-6F D' - Seq. No.: 00062 A/S Pos.: — Date: 10/01/97
Replicate 1 Time: 10:47
Peak Area (A-s): 0.022 Peak Height (A): 0.001
Blank Corrected Pk Height (A): 0.001
Concentration (ug/L ): 0.024
Hg2 ID: 183-3-8C Seq. No.: 00063 A/S Pos.: — Date: 10/01/97
Sample abs. is greater than that of the largest standard. tc\«L V Seq. No.: 00065 A/S Pos.: — Date: 10/01/97
*&it-4Wte
Replicate 1 Time: 11:01
Peak Area (A-s): 6.070 Peak Height (A): 0.258
Blank Corrected Pk Height (A): 0.258
Concentration (ug/L ): 6.868
Hg2 ID: 183-3-8D Seq. No.: 00066 A/S Pos.: — Date: 10/01/97
Replicate 1 Time: 11:02
Peak Area (A-s): 0.886 Peak Height (A): 0.037
Blank Corrected Pk Height (A): 0.037
Concentration (ug/L ): 0.990
r ^
V -/
Hg2
ID: 183-3-8D D
Replicate 1
Peak Area (A-s): 0.856
Seq. No.: 00067 A/S Pos.: — Date: 10/01/97
Time: 11:04
Peak Height (A): 0.037
-------
- 31ank Corrected Pk Height (A): 0.037
Concentration (ug/L ): 0.974
L.
Hg2
ID: 183-3-8E
Seq. No.: 00068 A/S Pos.: -- Date: 10/01/97
I Replicate 1
Peak Area (A-s): 0.539
, Blank Corrected Pk Height (A): 0.023
j Concentration (ug/L ): 0.620
Time: 11:05
Peak Height (A): 0.023
Hg2 ID: 183-3-8E D
Seq. No.: 00069 A/S Pos.: — Date: 10/01/97
Replicate 1
• •Peak Area (A-s): 0.544
\ 31ank Corrected Pk Height (A): 0.023
"Concentration (ug/L ): 0.615
Time: 11:06
Peak Height (A): 0.023
-vlg2 ID: 183-3-8E MS
Seq. No.
00070
A/S Pos.: —
Replicate 1
>eak Area (A-s): 4.298
Blank Corrected Pk Height (A): 0.184
Concentration (ug/L ): 4.902
Time: 11:07
Peak Height (A): 0.184
Date: 10/01/9'
Hg2
ID: 183-3-8E USD
Seq. No.: 00071 A/S Pos.: — Date: 10/01/97
••teplicate 1
Peak Area (A-s): 4.180
Jlank Corrected Pk Height (A): 0.181
'.oncentration (ug/L ): 4.830
Time: 11:08
Peak Height (A): 0.181
Ig2 ID: CCV3=6.0ug/L
Seq. No.: 00072
A/S Pos.: —
, Replicate 1
1 'eak Area (A-s): 0.038
< Jlank Corrected Pk Height (A): 0.002
Concentration (ug/L ): 0.043
Time: 11:09
Peak Height (A): 0.002
Date: 10/01/9
Hg2 ID: CCV3=6.0ug/L
Seq. No.: 00073 A/S Pos.: — Date: 10/01/97
leplicate 1
"~Peak Area (A-s): 4.570
.Blank Corrected Pk Height (A): 0.194
1 oncentration (ug/L ): 5.162
Time: 11:11
Peak Height (A): 0.194
( ,g2 ID: CCB3
Seq. No.: 00074
A/S Pos.: —
Replicate 1
r"eak Area (A-s): 0.017
! lank Corrected Pk Height (A): 0.001
""Concentration (ug/L ): 0.019
Time: 11:12
Peak Height (A): 0.001
Date: 10/01/97
362
-------
Hg2 ID: 183-3-8F
Seq. No.: 00075 A/S Pos.: -- Date: 10/01/97
Replicate 1
Peak Area (A-s): 0.048
Blank Corrected Pk Height (A): 0.002
Concentration (ug/L ): 0.059
Time: 11:13
Peak Height (A): 0.002
Hg2 ID: 183-3-8F D
Seq. No.: 00076 A/S Pos.: — Date: 10/01/97
Replicate 1
Peak Area (A-s): 0.103
Blank Corrected Pk Height (A): 0.004
Concentration (ug/L ):• 0.112
Time: 11:14
Peak Height (A): 0.004
Hg2 ID: CCV4=6.0ug/L
Seq. No.: 00077 A/S Pos.: -- Date: 10/01/9
Replicate 1
Peak Area (A-s): 4.850
Blank Corrected Pk Height (A): 0.207
Concentration (ug/L ): 5.507
Time: 11:15
Peak Height (A): 0.207
Hg2 ID: CC84
Seq. No.: 00078 A/S Pos.: — Date: 10/Oi/?-
Replicate 1
Peak Area (ft-s): 0.01S
Blank Corrected Pk Height t'AJ: 0.001
Concentration (ug/L ): O.Olfr
Time: ii:io .
Peak Height (A.); 0.001
-------
\ ID/Weight File: AB815.IDW
Sample Volume: 100 mL
•'
i Loc. Sample ID
0 STD BLK
( 1 STDl=0.2ug/L
I 2 STD2=0.5ug/L
3 STD3=1.0ug/L
4 STD4=2.0ug/L
! 5 STD5=5.0ug/L
^ 6 STD6=10.0ug/L
7 ICV=4.0ug/L
I 8 ICB
9 CHECK
10 43231 MB
11 43231 MB3. D
L 12 43231 LCS
13 43231 LCS
f 14 184-23-1AB
' 15 184-23-1A6 D
16 184-23-1AB
; 17 184-23-1AB HSD
18 184-23-2AB
19 184-23-2AB D
20 CCVl=6.0ug/L
21 CCB1
|_ 22 184-23-3AB
23 184-23-3AB D
/ - 24 184-23-4AB
25 184-23-4A8 D
26 184-23-6AB
27 184-23-6AB D
28 184-23-7AB
29 184-23-7AB D
30 184-23-8AB
' 31 184-23-8AB D
32 CCV2=6.0ug/L
33 CCB2
34 184-23-9AB
35 184-23-9AB D
36 CCV3=6.0ug/L
37 CCB3
Analyst: RICHARDS
Nominal Weight: 1.0 g
-H
Weight
Dilution
3-02,0-1 (o
1-02,0-2^
I
L
364
-------
Element File: HG_.MEL
Element: Hg2
Print Data: Main+Suppl
Print: Calib. Curve
Remarks:
STANDARDS= 3-020-1
QC= 3-020-2
Analyst: RICHARDS
Peak Storage: None
INSTRUMENT: 5100
Wavelength: 253.7 Peak
Signal Type: AA
Read Time: 30.0
Sample Replicates: 1
Standard Replicates: 1
Technique: MHS Version: 7.01
Slit: 0.7 Low
Signal Measurement: Peak Height (5)
Read Delay: 1.0 60C Time: 2
FLAME:
Flame Type: Air
Oxidant Flow: 10.0 L/min
Flame Sensor: On
Fuel Flow: 2.0 L/min
CALIBRATION:
Solutions
ft « 1 -i W Q 1 -?a « L/
(-.aiiD, clank
Standard 1
Standard 2
Standard 3
Standard 4
Standard 5
Standard 6
Calibration
Calibration
i
•
i
i
i oxr**
i b 1 U
ISTD
ISTD
ISTD
!STD
;STD
ISTD
Units
Type:
ID
D 1 I/
fcjLK
1
2
w
4
5
6
: ug/L
Linear
Cone I
i
_ _ _ i
i
0.2001
o.sooi
1.000!
2.000J
5.000J
10.000!
Sample Units:
ug/-L
QC:
Matrix Check Calculations:
% Difference for Dupls: No
% Recovery for Spike: No
Locations:
Locations:
Cone:
365
-------
'Element File: HG_.MEL Element: Hg2 Wavelength: 253.7
,-Oate: 10/06/97 Time: 12:47 Slit: 0.7 L
< fata File: AB815.DAT ID/Wt File: AB815.IDW Lamp Current: O
-technique: 'MHS Calib. Type: Linear Energy: 71
Remark 1: STANDARDS= 3-020-1
( '.emark 2: QC= 3-020-2
f'1g2 ID: STD BLK Seq. No.: 00003 A/S Pos. : — Date: 10/06/97
Replicate 1 Time: 12:48
, Peak Area (A-s): -0.000 Peak Height (A): 0.000
I lank Corrected Pk Height (A): 0.000
Concentration (ug/L ): 0.003
! iuto-zero performed.
i
f'g2 ID: STDl=0.2ug/L Seq. No.: 00004 A/S Pos.: -- Date: 10/06/97
""Replicate 1 Time: 12:49
;Peak Area (A-s): 0.123 Peak Height (A): 0.005
I lank Corrected Pk Height (A): O.OO5
Concentration (ug/L ): 0.121
i ;tandard number 1 applied. [0.200]
L orrelation coefficient: l.OOOOO Slope: 0.0231
~-,. ,~.
' g2 ID: STD2=0.5ug/L Seq. No.: 00005 A/S Pos.: -- Date: 10/06/97
i.
Cample abs. is greater than that of the largest standard.
\ eplicate 1 Time: 12:51
^,-eak Area (A-s): 0.335 Peak Height (A): O.013
Blank Corrected Pk Height (A): 0.013
' oncentration (ug/L ): 0.565
Standard number 2 applied. [O.500]
/Correlation coefficient: 0.99473 Slope: 0.0257
,Hg2 ID: STD3=1.0ug/L Seq. No.: 00006 A/S Pos.: -- Date: 10/O6/97
Cample abs. is greater than that of the largest standard.
Replicate 1 Time: 12:52
eak Area (A-s): 0.708 Peak Height (A): 0.028
,_ lank Corrected Pk Height (A): 0.028
Concentration (ug/L ): 1.073
; tandard number 3 applied. [1.000]-
"Correlation coefficient: 0.99763 Slope: 0.0272
^ ~ , ., ~, .. , ,~~~~ ,~~, . , . , ,«,«. , _,
v,g2 ID: STD4=2.0ug/L Seq. No.: 00007 A/S Pos.: -- Date: 10/06/97
I ample abs. is greater than that of the largest standard.
|_eplicate 1 Time: 12:53
Peak Area (A-s): 1.570 Peak Height (A): 0.063
366
-------
'Blank Corrected Pk Height (A): 0.063
Concentration (ug/L ): 2.321
r i
Standard number 4 applied. [2.00O]
Correlation coefficient: 0.99425 Slope: 0.0306
~~~^^~~~~~~~~~~~~^^^^~^^~~~~~~~~~~~~~~~~~~~~~^~^~^^^^~~~~^~^~~^~,v,~~~~~~~~~~~~..' ~\
Hg2 ID: STD5=5.0ug/L Seq. No.: 00008 A/S Pos.: — Date: 10/06/9V
Sample abs. is greater than that of the largest standard. f'
Replicate 1 -.-. Time: 12:54 ^_
Peak Area (A-s): 4.273 Peak Height (A): 0.179
Blank Corrected Pk Height (A): 0.179 n
Concentration (ug/L ): 5.851
V j
Standard number 5 applied. [5.000] ^
Correlation coefficient: 0.99610 Slope: 0.0350
Hg2 ID: STD6=10.Oug/L Seq. No.: 00009 A/S Pos.: -- Date: 10/O6/9"
\
Sample abs. is greater than that of the largest standard.
Replicate 1 Time: 12:55
Peak Area (A-s): 8.685 Peak Height (A): 0.365
Blank Corrected Pk Height (A): 0.365
Concentration (ug/L ): 10.425
Standard number 6 applied. [10.0OO]
Correlation coefficient: 0.99891 Slope: 0.0362
367
-------
Element File: HG_.MEL
,-Date: 10/06/97
I Data File: AB815.DAT
^-Technique: MHS
Remark 1: STANDARDS= 3-020-1
1 Remark 2: QC= 3-020-2
Element: Hg2
Time: 12:56
ID/Wt File: AB815.IDW
Calib. Type: Linear
Wavelength: 253.7
Slit: 0.7 L
Lamp Current: 0
Energy: 71
r-
H
Display Calibration - C; WjSER\flflJ I LES\ELEHEHT\HG..HEL
0.365-
Lineap
COPP. Coef.: B.99B91
Slope: 0.0362
Concentration
18.
368
-------
Element File: HG_.MEL
Date: 10/06/97
Data File: AB815.DAT
Technique: MHS
Remark 1: STANDARDS= 3-020-1
Remark 2: QC= 3-020-2
Element: Hg2
Time: 12:57
ID/Wt File: AB815.IDW
Calib. Type: Linear
Wavelength: 253.7
Slit: 0.7 L
Lamp Current: 0
Energy: 71
Hg2 ID: ICV=4.0ug/L
Seq. No.: 00010 A/S Pos.: -- Date: 10/06/9^
Replicate 1
Peak Area (A-s): 3.724
Blank Corrected Pk Height (A): 0.158
Concentration (ug/L ): 4.374
Time: 12:58
Peak Height (A): 0.158
Hg2
ID: ICB
Seq. No.: 00011
A/S Pos,
Date: 10/06/9'
Replicate 1
Peak Area (A-s): 0.008
Blank Corrected Pk Height (A): O.OOO
Concentration (ug/L ): 0.011
Hg2
ID: CHECK LO
Nc
Replicate i
Peak Area (A-s): 0.093
Blank Corrected Pk Height (A): 0.004
Concentration (ug/L ): O.O97
Time: 13:00
Peak Height (A): 0.000
000.12 A/£ Pos.: -- Dste: 10/06/9
Time: 13:02
Peal* Hei an t f A ): 0. OO4
•Hg:
ID: 43231 MB£
Seq. Nc. : 0001;
Peplicats 1
Peak Area (A-si: 0.009
Slank Corrected Pk Height (A): O.OOO
Concentration (ug/L ): 0.000
A/S Pos.: —
Date: lO/06/9~
Time: 13:03
Peak Height (A): 0.000
Hg2
ID: 43231 MBZ D
Seq. No.: 00014
Replicate 1
Peak Area (A-s): 0.005
Blank Corrected Pk Height (A): O.OOO
Concentration (ug/L ): 0.006
A/S Pos.: —
Date: 10/06/9"?,
Time: 13:04
Peak Height (A): O.OOO
Hg2
ID: 43231 LCS
Seq. No.: 00015
Replicate i
Peak Area (A-s): 3.826
Blank Corrected Pk Height (A): O.172
Concentration (ug/L ): 4.748
A/S Pos.: --
Date: 10/06/9~
Time: 13:05
Peak Height (A): 0.172
Hg2
ID: 43231 LCSi D
Seq. No.: 00016
A/S Pos.: --
Date: 10/06/97
369
-------
I Replicate 1
Peak Area (A-s): 4.141
("Blank Corrected Pk Height (A): 0.178
j Concentration (ug/L ): 4.928
Time: 13:06
Peak Height (A): 0.178
Hg2
ID: 184-23-1AB
Seq. No.: 00017
Replicate 1
Peak Area (A-s): 4.484
v_Blank Corrected Pk Height (A):. 0.191
Concentration (ug/L ): 5.269
A/S Pos.: —
Date: 10/06/97
Time: 13:07
Peak Height (A): 0.191
Hg2 ID: 184-23-1AB D
Seq. No.: 00018
Replicate 1
Peak Area (A-s): 4.343
Blank Corrected Pk Height (A): O.186
Concentration (ug/L ): 5.153
A/S Pos.: --
Date: 10/06/97
Time: 13:08
Peak Height (A): 0.186
i Hg2 ID: 184-23-1AB MS
Seq. No.: OO019
A/S Pos. : --
Date: 10/06/9^
Replicate 1
Peak Area (A-s): 8.967
Blank Corrected Pk Height (A): 0.383
Concentration (ug/L ): 10.592
Time: 13:09
Peak Height (A): 0.383
I Hg2
ID:
134
-23-1ABMSDX2
Seq.
No. :
00020
A/S
Pos . : --
Date :
10/O6/9-
Replicate 1
Peak Area (A-s): 4.728
Blank Corrected Pk Height (A):
Concentration (ug/L ): 5.561
0.201
Time: 13:18
Peak Height (A): 0.201
Hg2
ID: 184-23-1ABMSDX2
Seq. No.: OO021
Replicate 1
Peak Area (A-s): 4.121
Hank Corrected Pk Height (A): 0.177
Concentration (ug/L ): 4.881
A/S Pos.: --
Date: 10/O6/9T'
Time: 13:19
Peak Height (A): 0.177
ID: 184-23-2AB
Seq. No.: 00022
Replicate 1
< 'eak Area (A-s): 7.587
i Jlank Corrected Pk Height (A): 0.33S
Concentration (ug/L ): 9.249
A/S Pos.: --
Time: 13:21
Peak Height (A): 0.335
Date: 10/06/97
"Hg2
ID: 184-23-2AB D
Seq. No.: O0023
\ leplicate 1
L..>eak Area (A-s): 7.506
Blank Corrected Pk Height (A): 0.329
A/S Pos.: —
Time: 13:22
Peak Height (A): 0.329
370
Date: 10/06/97
-------
Concentration (ug/L ): 9.097
Hg2 ID: CCVl=6.0ug/L
Seq. No.: 00024
Replicate 1
Peak Area (A-s): 5.358
Blank Corrected Pk Height (A): 0.230
Concentration (ug/L ): 6.357
A/S Pos.: --
Time: 13:22
Peak Height (A): 0.230
Date: 10/06/9,
r i-
Hg2
ID: CCB1
Seq. No.: 00025 A/S Pos.: — Date: 10/06/97,
Replicate 1
Peak Area (A-s): 0.053
Blank Corrected Pk Height (A): 0.002
Concentration (ug/L ): 6.047
Time: 13:23
Peak Height (A): O.002
Hgi
ID: 184-23-3AB
Seq. No.: 00026
Replicate 1
Peak Area (A-s): 5.790
Blank Corrected Pk Height (A): 0.251
Concentration (ug/L ): 6.931
A/S Pos.: -- Date: 10/06/9"
Time: 13:24
Peak Height (A): O.251
Hg2
ID: 184-23-3AB D
Seq. No.: 00027
Replicate 1
Peak Area (A-s): 5.473
Blank Corrected Pk Height (A): 0.234
Concentration (ug/L ): 6.479
A/S Pos.: --
Time: 13:26
Peak Height (A): 0.234
Date: 10/06/9''
Hg2 ID: 184-23-4AB
Seq. No.: 00028
Replicate 1
Peak Area (A-s): 0.021
Blank Corrected Pk Height (A): 0.001
Concentration (ug/L ): 0.014
A/S Pos.: --
Time: 13:30
Peak Height (A): 0.001
Date: !O/06/97r
Hg2
ID: 184-23-4AB D
Seq. No.
Replicate 1
Peak Area (A-s): 0.016
Blank Corrected Pk Height (A): 0.000
Concentration (ug/L ): 0.011
00029
A/S Pos.: --
Time: 13:31
Peak Height (A): 0.000
Date: 1O/06/9?
Hg2
ID: 184-23-6AB
Seq. No.: 0003O
Replicate 1
Peak Area (A-s): O.O80
Blank Corrected Pk Height (A): O.003
Concentration (ug/L ): 0.092
A/S Pos.: --
Time: 13:32
Peak Height (A): O.OO3
Date: 10/06/97 r
-------
Hg2
ID: 184-23-6AB D
Seq. No.: OO031
A/S Pos.: —
Date: 10/06/97
; splicate 1
v eak Area (A-s): 0.078
Blank Corrected Pk Height (A): 0.003
i Dncentration (ug/L ): 0.083
Time: 13:33
Peak Height (A): 0.003
'32
ID: 184-23-7AB
Seq. No.: 00032
A/S Pos.: —
Date: 10/06/97
Replicate 1
Peak Area (A-s): 0.034
I lank Corrected Pk Height (A): 0.001
Loncentration (ug/L ): 0.033
Time: 13:34
Peak Height (A): 0.001
1.32
ID: 184-23-7AB D
Seq. No.: OO033
A/S Pos.: --
Date: 10/06/9-*
"splicate 1
I sak Area (A-s): 0.032
blank Corrected Pk Height (A): 0.002
ppncentration (ug/L ): 0.042
Time: 13:35
Peak Height (A): 0.002
Hg2 ID: 184-23-8AB
Seq. No.: OO034
[_eplicate 1
Peak Area (A-s): 0.041
.^lank Corrected Pk Height (A): 0,001
oncentration (ug/L ): 0.036
A/S Pos.: --
Time: 13:36
Peak Height (A): 0.001
Date: 10/06/97
ID: 184-23-8AB D
Seq. No.: 00035
A/S Pos.: --
Replicate 1
| eak Area (A-s): 0.041
lank Corrected Pk Height (A): 0.001
Concentration (ug/L ): 0.036
Time: 13:37
Peak Height (A): 0.001
Date: 10/06/97
ID: CCV2 = 6.0ug/L
Seq. No.: 00036
J eplicate 1
-,-eak Area (A-s): 5.261
Blank Corrected Pk Height (A): 0.229
[ oncentration (ug/L ): 6.329
A/S Pos.: --
Time: 13:38
Peak Height (A): 0.229
Date: 10/06/97
:"g2
ID: CCB2
Seq. No.: OO037 A/S Pos.: --
Replicate 1
Peak Area (A-s): 0.029
[ lank Corrected Pk Height (A): 0.001
Concentration (ug/L ): 0.025
Date: 10/06/9:
Time: 13:39
Peak Height (A): 0.001
r
L.92
ID: 184-23-9AB
Seq. No.: OO038 A/S Pos.: -- Date: 10/06/97
L
372
-------
Replicate 1
Peak Area (A-s): 0.018
•Blank Corrected Pk Height (A): 0.000
Concentration (ug/L ): O.006
Time: 13:40
Peak Height (A): 0.000
Hg2
ID: 184-23-9AB D
Seq. No.: 00039
A/S Pos.: --
Date: 10/06/97
Replicate 1
Peak Area (A-s): 0.012
Blank Corrected Pk Height (A): Q.OOO
Concentration (ug/L ): 0.003
Time: 13:40
Peak Height (A): O.OOO
n
Hg2 ID: CCV3=6.0ug/L
Seq. No.: 00040
Replicate 1
Peak Area (A-s): 5.205
Blank Corrected Pk Height (A): 0.219
Concentration (ug/L ): 6.046
A/S Pos.: --
Date: 10/06/97-'
Time: 13:41
Peak Height (A): 0.219
Hg2
ID: CCB3
Seq. No.: 00041
Replicate 1
Peak Area (A-s): 0.034
Blank Corrected Pk Height (A): O.OO2
Concentration (ug/L ): 0.042
A/S Pos.: --
Date: 10/06/9T
Time: 13:42
Peak Height (A): 0.002
373
-------
i D/Weight File: A8816.IDW
-oample Volume: 100 mL
Analyst: RICHARDS
Nominal Weight: 1.0 g
. Loc,
O
1
2
3
4
5
6
7
- a
9
10
11
12
13
14
15
16
17
IS
19
2O
21
22
23
24
25
26
27
28
29
3O
31
32
33
34
35
36
37
38
39
4O
41
42
43
44
45
46
47
48
49
50
51
52
53
L
Sample ID
STD BLK
STDl=0.2ug/L
Weight
Dilution
STD3=1.0ug/L
STD4=2.0ug/L
STD5=5.0ug/L
STD6=10.0ug/L
ICV=4.0ug/L
ICB
CHECK l_o£^ „.
43231 MB4
43231 MB^l D
43231 LCS4
43231.LCS4 D
184-25-5^10^8
1 S3- 15-10 •$.*'
' 183- 15- IF D* '«(<-/«•»
183-15- l4c MS"1"^
183-1 5- 11
CCVl=6.0ug/L
CCB1
133-L5-1C
183-15-10 D
183-15-18
183-15-18 0
133- 15- IE
183-15-1E D
CCV2=6.0ug/L
CCB2
43271 MB!
43271 MB1 D
43271 LCS1
43271 LCS1
183-43-1AB
183-43-1AB D
183-43-1C
183-43-1C D
183-43- 1C MS
183-43-1C MSD
CCVl=6.0ug/L
CCB1
183-43-10
183-43-1D D
183-43-1E
183-43-1E D
183-43-1F
183-43-1F D
183-43-2AB
183-43-2AB D
183-43-3A8
183-43-3AB D
CCV2=6.0ug/L
CCB2
•*•
374
-------
Loc. Sample ID Weight Dilution
54 IS3-43-2D
55 183-43-2D D
56 183-43-2E -
57 . 183-43-2E D
58 ^~183-43-2C
59 183-43-2C D
60 1S3-43-2C MS
61 183-43-2C MSD ...
62 183-43-2F
63 183-43-2F D -^-02.0 -V- *&- <°AA?
64 CCV3 = 6.0ug/L S ^ ^ ' '
65 CC83
66 183-43-4BC
67 183-43-4BC D
68 183-43-30
69 183-43-30*
70 1S3-43-3E
71 183-43-3E D
72 183-4.3-3F
73 133-43-3F D
74 183-43-4A6
75 1S3-43-4A8 D
76 CCV4=6.0ug/L
77 CCB4
78 183-43-40
79 183-43-40 D
80 183-43-3C
81 183-43-3C D
82 133-43-3C MS
83 133-43-3C MSD
84 183-43-4E
85 183-43-4E D
86 L33-43-4F •> />•
87 183-45-4F D i To ^ *"l »
33 CCV5=6.0ug/L
89 CCB5
375
-------
Element Fil-e: HG_.MEL
Element: Hg2
Print Data: Main+Suppl.
Print: Calib. Curve
Remarks: .
STANDARDS= "3-020-3
-QC= 3
Analyst: RICHARDS
Peak Storage: None
10
f INSTRUMENT: 5100
{_ Wavelength: 253.7 Peak
Signal Type: AA
r Read Time: 3O.O
J Sample Replicates: 1
u Standard Replicates: L
Technique: MHS Version: 7.01
Slit: 0.7 Low
Signal Measurement: Peak Height (5)
Read Delay: 1.0 BOC Time: 2-
FLAME:
-Flame Type: Air
Oxidant Flow: 10.0 L/min
Flame.Sensor: On
Fuel Flow: 2.0 L/min
CALIBRATION:
Solutions ! ID
i
i
^ a 1 1 D . 6 JL a n K jblD 8 L ft
Standard 1 | STD 1
Standard 2 \ STD 2
Standard 3 ; STD 3
Standard 4 |STD 4
Standard 5 j STD 5
Standard 6 !STD 6
Calibration Units: ug/L
Calibration Type: Linear
Cone
— __.-._ —
0 . 200
0 . 500
1 . 000
2 . 000
5 . 000
10.000
Sample
} Units: ug/L
1C:
"Matrix Check Calculations:
<% Difference for Dupls: No
' ; Recovery for Spike: No
Locations:
Locations:
Cone;
L
376
-------
element File: HG_.MEL
Date: 10/08/97
Data File: AB816.DAT
Technique: MHS
Remark 1: STANDARDS- 3-020-3
Remark 2: QC= 3-020-4
Element: Hg2
Time: 09:47
ID/Wt File: AB816.IDW
Calib. Type: Linear
Wavelength: 253.7r,
Slit: 0.7 L
Lamp Current: O
Energy: 71
Hg2
ID: Seq. 00001
Seq. No.: 00001
A/S Pos.: --
Date: 10/08/ 7
Replicate 1
Peak Area (A-s): -0.026
Blank Corrected Pk Height (A): -0.001
Concentration (ug/L ): -0.061
Auto-zero performed.
Time: 09:47
Peak Height (A):
-0.001
Hg2 ID: Seq. 00002
Seq. No.: 00002
Replicate 1
Peak Area (A-s): 0.036
Blank Corrected Pk Height (A): 0.002
Concentration (ug/L ): 0.074
Auto-zero performed.
A/S Pos.: --
Date: 10/08/<
Time: 09:49
Peak Height (A): 0.002
Hg2
ID: STD BLK
Seq. No.: 00003
Replicate 1
Peak Area (A-s): -0.000
Blank Corrected Pk Height (A): -0.000
Concentration (ug/L ): -0.009
Auto-zero performed.
A/S Pos.: --
Date: 1O/08/9
Time: 09:52
Peak Height (A): -0.000
Hg2 ID: STDl=0.2ug/L
Seq. No.: OO004
A/S Pos.: —
Date: 10/08/9'
Sample abs. is greater than that of the largest standard.
Replicate 1 Time: 09:54
Peak Area (A-s): 0.166 Peak Height (A): 0.003
Blank Corrected Pk Height (A): 0.008
Concentration (ug/L ): 0.330
Standard number 1 applied. [0.200]
Correlation coefficient: 1.00000
Slope: 0.0381
Hg2 ID: STD2=0.5ug/L
Seq. No.: OOOO5 A/S PCS.: -- Date: 10/08/97rA
Replicate 1
Peak Area (A-s): -0.005
Blank Corrected Pk Height (A): 0.000
Concentration (ug/L ): 0.000
Time: 09:55
Peak Height (A): 0.000
377
-------
Hg2 ID: STD2=0.5ug/L
Seq. No.: 00006
A/S Pos.: —
Date: 10/O8/97
Sample abs. is greater than that of the largest standard.
Replicate 1 Time: 10:01
Peak Area (A-s): 0.449 Peak Height (A): 0.019
Blank Corrected Pk Height (A): 0.019
Concentration (ug/L ): 0.511
Standard number 2 applied. [0.500]
Correlation coefficient: 0.99984
Slope: O.0388
Hg2 ID: 3TD3=1.Oug/L
Seq. No. : 00007
A/S Pos.: --
Sample abs. is greater than that of the largest standard.
Replicate 1 Time: 10:02
Peak Area (A-s): 0.830 Peak Height (A): 0.035
Blank Corrected Pk Height (A): 0.035
Concentration (ug/L ): 0.912
Standard number 3 applied. [1-000]
, .Correlation coefficient: 0.99693
Slope: 0.0362
Date: 10/08/97
Hg2
ID: STD4r2.Oug/L
Seq. No.: 00008
A/S Pos.: --
Samole abs. is greater than that of the largest standard.
Replicate 1 Time: 10:03
Peak Area (A-s): 1.682 Peak Height (A): O.O72
Blank Corrected Pk Height (A): 0.072
Concentration (ug/L '): 1.991
Standard number 4 applied. [2.00O]
- Correlation coefficient: 0.99946
Slope: 0.0361
Date: 1O/08/9"
Hg2
ID: STD5=5.Oug/L
Seq. No.: 00009
A/S Pos.: --
Sample abs. is greater than that of the largest standard.
Replicate 1 Time: 10:05
Peak Area (A-s): 4.249 Peak Height (A): 0.187
Blank Corrected Pk Height (A): 0.187
Concentration (ug/L ): 5.171
Standard number 5 applied. [5.00O]
Correlation coefficient: 0.99977
Slope: 0.0371
Date: 10/08/97
Hg2 ID: STD6=10.Oug/L Seq. No.: 00010 A/S Pos.: —
Sample abs. is greater than that of the largest standard.
, Replicate 1
: Peak Area (A-s): 8.594
^-Blank Corrected Pk Height (A): 0.371
Concentration (ug/L ): 10.005
r
[_Standard number 6 applied. [10.000]
Correlation coefficient: 0.99995
Time: 10:06
Peak Height (A): 0.371
Slope: 0.0371
Date: 10/08/97
378
-------
Element File: HG_.MEL Element: Hg2
. Date: 10/08/97 Time: 10:06
Data File: A8816.DAT ID/Wt File: AB816.IDW
Technique: MHS Calib. Type: Linear
Remark 1: STANDARDS= 3-020-3
Remark 2: QC= 3-020-4
Wavelength: 253.7
Slit: 0.7 L
Lamp Current: O
Energy: 71
H| Display Calibration - C:\m.USER\ftflJILES\ELEMEHT\H6_.HEL
8.371n
0
*
JS5
Linear
Corn, Coef.: B.99995
Slope; 0.0371
Concentration
18.
379
-------
Hg2 ID: ICV=4.0ug/L
Seq. No.: 00011
A/S Pos.: —
Date: 10/08/97
Replicate 1
L-Peak Area (A-s): -3.457
Blank Corrected Pk Height (A): 0.151
[ Concentration (ug/L ): 4.078
Time: 10:09
Peak Height (A): 0.151
Hg2
ID: ICB
Seq. No.: 00012
Replicate 1
Peak Area (A-s): 0.008
alank Corrected Pk Height (A): 0.000
Concentration (ug/L ): 0.005
A/S Pos.: --
Date: 10/08/97
Time: 10:10
Peak Height (A): 0.000
Hg2
ID: CHECK LO
Seq. No,
Replicate 1
Peak Area (A-s): 0.173
Blank Corrected Pk Height (A): 0.007
Concentration (ug./L ): 0.200
00013
A/S Pos.: —
Date: 10/08/97
Time: 10:12
Peak Height (A): O.OO7
Hg2
ID: 43231
Sea. No.: 00014
A/S Pos.: --
Date: 10/08/97
Replicate 1
Peak Area (A-s): 0.014
Blank Corrected Pk Height (A): 0.000
Concentration (ug/L ): O.OO8
Time: 1O:13
Peak Height (A): 0.000
ID: 43231 MB? D
Seq. No.: 00015
Replicate 1
3eak Area (A-s): 0.016
Jlank Corrected Pk Height (A):
Concentration (ug/L ): 0.030
0.001
A/S Pos.: --
Date: 1O/08/97
Time: 1O:14
Peak Height (A): 0.001
~Hg2 ID: 43231 LCS/
•
Seq. No.: 00016 A/S Pos.: --
Date: 1O/08/97
j Jeplicate 1
i-"eak Area (A-s): 4.642
Blank Corrected Pk Height (A): 0.205
I :oncentration (ug/L ): 5.526
Time: 10:16
Peak Height (A): 0.205
'92
ID: 43231 LCS4* D
^Sf \\-A-VlCC
Replicate 1
,°eak Area (A-s): 4.397
i 'lank Corrected Pk Height (A): 0.188
^concentration (ug/L ): 5.053
Seq. No.: 00017
A/S Pos.: --
Date: 1O/O8/97
Time: 10:17
Peak Height (A): 0.188
-g2 ID: 184-2^-5^
Seq. No.: 00018
A/S Pos.: --
Date: 10/08/97
330
-------
-Re01"icate 1
Peak Area (A-s): 0.024
•Blank Corrected Pk Height (A): 0.001
Concentration (ug/L ): 0.035
Time: 10:18
Peak Height (A): 0.001
Hg2
ID: 134-22-5710AB,
Seq. No.: 00019
Replicate 1
Peak Area (A-s): 0.019
Blank Corrected Pk Height (A):- 0.001
Concentration (ug/L ): 0.022
A/S Pos.: —
Date: 10/O8/9'
Time: 10:19
Peak Height (A): 0.001
Hg2
ID: 1 83 -lfc-
Seq. No.: 00020
Replicate 1
Peak Area (A-s): 0.051
Blank Corrected Pk Height (A): 0.002
Concentration (ug/L ): 0.054
A/S Pos.: --
Date: 10/08/9/-
Time: 10:20
Peak Height (A): 0.002
Hg2
ID: 183-15-lK»
Seq. No,
Replicate 1
Peak Area (A-s): 0.035
Blank Corrected Pk Height (A): 0.002
Concentration (ug/L ): 0.043
OO021
A/S Pos.: --
Date: 10/03/97
Time: 10:21
Peak Height (A): 0.002
Hg2
ID: 183-15-lV'MS
Seq. No,
Replicate 1
Peak Area (A-s): 4/723
Blank Corrected.Pk Height (A): 0.217
Concentration (ug/L ): 5.842
00022
A/S Pos.: --
Date: 10/08/97^.
Time: 10:22
Peak Height (A): 0.217
Hg2
ID: 183-15-
MSD
Seq. No.: OO023
Replicate 1
Peak Area (A-s): 4.373
Blank Corrected Pk Height (A):
Concentration (ug/L ): 5.105
0.190
A/S Pos.: --
Time: 10:23
Peak Height (A): 0.190
Date: 10/08/97
Hg2
ID: CCVl=6.0ug/L
Seq. No.: 00024
A/S Pos.: --
Replicate 1
Peak Area (A-s): 5.210
Blank Corrected Pk Height (A): 0.234
Concentration (ug/L ): 6.298
Time: 10:24
Peak Height (A): 0.234
Date: 1O/08/97
Hg2
ID: CCB1
Seq. No.: OOO25
A/S Pos.: --
Replicate 1
Peak Area (A-s): 0.016
Blank Corrected Pk Height (A): 0.001
Time: 1O:25
Peak Height (A): 0.001
Date: 1O/08/97'
381
-------
Concentration (ug/L ): 0.019
r
Hg2
ID: 183-15-1C
Seq. No.: 00026
Replicate 1
(Peak Area (A-s): 0.000
• Blank Corrected Pk Height (A): 0.000
Concentration (ug/L ): 0.005
A/S Pos.: —
Time: 10:26
Peak Height (A): 0.000
Date: 10/08/97
L
Hg2
ID: 183-15-1C D
Seq. No.: 00027
Replicate 1
Peak Area (A-s): 0.007
Blank Corrected Pk" Height (A): 0.000
Concentration (ug/L ): 0.008
A/S Pos.: —
Time: 10:27
Peak Height (A): 0.000
Date: 10/08/97
, Hg2 ID: 183-15-1B
Seq. No.: 00028
^Replicate 1
Peak Area (A-s): -0.007
; Blank Corrected Pk Height (A): -0.000
I Concentration (ug/L .) : -0.003
A/S Pos..: --
Date: 1O/08/97
Time: 10:23
Peak Height (A): -O.OOO
Hg2
ID: 183-15-1B D
Seq. No.: 00029
r Replicate 1
i Peak Area (A-s): -O.002
Blank Corrected Pk Height (A): -O.OOO
Concentration (ug/L ): -0.003
A/S Pos.: --
Date: 10/08/97
Time: 10:29
Peak Height (A-):
-O.OOO
Hg2 ID: 183-15-1E
Seq. No.: 00030
A/S Pos.: —
Date: 10/08/97
Replicate 1
Peak Area (A-s): -0.009
i 31ank Corrected Pk Height (A): 0.000
Concentration (ug/L ): 0.003
Time: 10:30
Peak Height (A): O.OOO
ID: 183-15-1E D
Seq. No.: 00031
Replicate 1
' ^eak Area (A-s): -0.016
; Blank Corrected Pk Height (A): -0.000
Concentration (ug/L ): -0.005
A/S Pos.: —
Date: 10/08/97
Time: 10:31
Peak Height (A)
-0.000
Hg2 ID: CCV2=6.Oug/L
Seq. No.: OOO32
I Replicate i
Weak Area (A-s): 4.569
Blank Corrected Pk Height (A): 0.201
{ Concentration (ug/L ): 5.404
A/S Pos.: —
Date: 10/08/97
Time: 1O:33
Peak Height (A): 0.201
382
-------
Hg2
ID: CC82
Seq. No.: 00033 A/S Pos.: -- Date: 10/08/S
Replicate 1
Peak Area (A-s): -0.006
Blank Corrected Pk Height (A): 0.000
Concentration (ug/L ): 0.000
Time: 10:34
Peak Height (A): 0.000
Hg2
ID: 43271 MB1
Seq. No.: 00034
Replicate 1
Peak Area (A-s): -0.007
Blank Corrected Pk Height (A): -0.000
Concentration (ug/L ): -0.003
A/S Pos.: --
Date: 10/08,
Time: 10:35
Peak Height (A):
-0.000
Hgi
ID: 43271 MB1 D
Seq. No.: 00035 A/S Pos.: — Date: 10/08/9'
Replicate 1
Peak Area (A-s): -0.014
Blank Corrected Pk Height (A): -0.000
Concentration (ug/L ): -0.011
Time: 10:36
Peak Height (A):
-0.000
Hg2
ID: 43271 LCS1
Seq. No.: 00036
Replicata 1
Peak Area (A-s): 4.426
Blank Corrected Pk Height (A): 0.192
Concentration (ug/L ): 5.175
A/S Pos.: --
Time: 10:37
Peak Height (A): 0.192
Date: 10/08/
Hg2 ID: 43271 LCS1
Seq. No.: 00037
Replicate 1
Peak Area (A-s): 4.192
Blank Corrected Pk Height (A): 0.182
Concentration (ug/L ): 4.913
A/S Pos.: --
Time: 10:38
Peak Height (A): 0.182
Date: 1O/Q8/9T
r '
Hg2
ID: 183-45-1AB
Seq. No,
Replicate 1
Peak Area (A-s): 0.033
Blank Corrected Pk Height (A): 0.001
Concentration (ug/L ): 0.035
00038
A/S Pos.: —
Time: 10:39
Peak Height (A): 0.001
Date:
Hg2
ID: 183-43-1AB D
Seq. No.: OO039
Replicate 1
Peak Area (A-s): 0.017
Blank Corrected Pk Height (A): 0.001
Concentration (ug/L ): 0.030
A/S Pos.: --
Time: 10:41
Peak Height (A): 0.001
Date: 1O/08/9;
Hg2 ID: 183-43-1C
Seq. No.: 00040
A/S Pos.: --
Date: 10/08/9:
38*
-------
f
ID/Weight File: AB818.IDW
•Sample Volume:"100 ml_
Loc.
i
« Sample ID
"o-
1
,2
V
4
5
6
- 7
8
9
10
11
12
13
14
15
16
17
18 '
19
20
21
22
23
24
25
26
27
28
29
3O
31
32
33
34
35
36
37
33
39
40
41
42
43
44
45
46
47
48
.49
50
51
52
53
STD BLK
STDl=0.2ug/L x.
STD2=0.5ug/L
STD3=1.0ug/L
STD4=2.0ug/L
STD5=5.0ug/L /
STD6=10.0ug/L
ICV = 4.0ug/l ~-
ICB
CHECK LO *o«>y
43271 MB-f -*"***
43271 MB-k D
43271 LCSB
43271 LCSJi D
133-43-8A3
183-43-3AB D
133-43-8C
183-43-8C D
133-43-SC MS
<• 1S3-43-8C MSD
CCVl=6.0ug/L _
CC81
183-43-8D
183-43-80 D
183-43-8E
183-43-8E D
183-43-8F
183-43-8F D
183-43-9AB
183-43-9AB D
1S3-43-9C
' 183-43-9C D
CCV2-6.0ug/l
CC82
183-43-90
133-43-9D D
183-43-96
183-43-9E D
183-43-9F
183-43-9F D
183-43-10A8
183-43- 10AB D
183- 43 -IOC
183-43-10C D
CCV3=6.0ug/L _
CCB3
183-43- 10D
183-43-10D D
183-43-10E
183-43-10E D
183-43-10F
183-43-1QF D
183-43-11C
183-43-11C D
Analyst: RICHARDS
Nominal Weight: 1.0 g
Weight
Dilution
3-02,0- 7
•V.OT.O-
3-
384
-------
Loc,
Sample 'ID
Weight
Dilution
54 1Q3-43-11C MS
55 18*3-43-110 MSD
'56 CCV4=6.0ug/L -
57 CCB4
5'3 183-43-11A6
39, 183-43-11A8 D
60 CCV5=6.0ug/L
61 CC85
62 43231 MB.
63 43231 MB!
64 43231
65 43231
66 183-3-1BC
67 183-3-1BC D
68 183-3-18C MS
69 183-3-1BC MSD
70 183-3-58C
71 183-3-5BC D
72 CCV6=6.0ug/L
73 CCB6
385
-------
Element File: HG_,MEL
Element: Hg.2
Print Data: Main+Suppl
Print: Cali^. Curve
Remarks:
STANDARDS^ 3-020-7
QC= 3-020-8
Analyst: RICHARDS
Peak Storage: None
INSTRUMENT: 5100
Wavelength: 253.7 Peak
Signal Type:" AA
Read Time: 30.0
Sample Replicates: 1
Standard Replicates: 1
Technique: MHS
Slit: 0.7 Low
Signal Measurement:
Read Delay: 1.0
Version: 7.01
Peak Height (5)
80C Time: 2
FLAME:
Flame Type: Air
Oxidant Flow: 1O.O L/min
Flame Sensor: On
Fuel Flow: 2.0 L/min
'CALIBRATION:
Solutions ! ID
i
i
caiio. Blank , biD 8L!\
Standard 1 !STD 1
Standard 2 |STD 2
Standard 3 ! STD 3
Standard 4 • | STD 4
Standard 5 | STD 5
Standard 6 |STD 6
Calibration Units: ug/L
Calibration Type: Linear
Cone •
0 . 200
0 . 500
1 . 000
2 . 000
5 . 000
10.00O
Sample
i Units: ug/L
QC:
"latrix Check Calculations:
"% Difference for Dupls: No
% Recovery for Spike: No
Locations:
Locations:
Cone.
•**.
336
•L
-------
Element File: HG_.M£L
Date: 10/10/97
Data File: AB818.DAT
Technique: ffHS
Remark 1:. STANDARDS= 3-020-7
Remark 2: QC= 3-O20-3
Element: -Hg2
Time: 13:51
ID/Wt File: AB818.IDW
Calib. Type: Linear
Wavelength:- 253.7
Slit: 0.7 L
Lamp Current: 0
Energy: 71
. ID: STD 8LK
Seq. No.: OOOO3
Replicate 1
Peak Area (A-s): -0.004
Blank Corrected Pk Height (A): -0.000
Concentration (ug/L. ): -0.005
Auto-zero performed.
A/S Pos.: —
Date: 10/LO/9T
Time: 13:52
Peak Height (A):
-0.000
Hg2 ID: STDl=0.2ug/L
Seq. No.: O0004
A/S Pos.: --
Replicate L
Peak Area (A-s): 0.156
Blank Corrected Pk Height (A): 0.006
Concent-ration (ug/L ): O.171
Standard number 1 applied. CO.200]
Correlation coefficient: 1.00000
Time: 13:53
Peak Height (A): O.OO6
Slope: 0.03
Date: 10/10/97
Hg2 ID: STD2=0.5ug/L
Seq. No.: 00005
A/S Pos.: --
Date: 10/10/97,,
Sample abs. i-s greater than that of the largest standard.
Replicate 1 Time: 13:54
Peak Area (A-s): 0.434 Peak Height (A): 0.018
Blank Corrected Pk Height (A): O.O18
Concentration fug/L ): 0.566
Standard number 2 applied. [0.500]
Correlation coefficient: O.99467
Slope: 0.0358
Hg2 ID: STD3=1.0ug/L
Seq. No.: OOOO6
A/S Pos.: --
Sample abs. is greater than that of the largest standard.
Replicate 1 Time: 13:55
Peak Area (A-s): O.S53 Peak Height (A): 0.035
Blank Corrected Pk Height (A): 0.035
Concentration (ug/L ;.- 0.989
Standard number 3 applied. [1.000J
Correlation coefficient: 0.99923 Slope: 0.0355
Date: 10/10/97
Hg2 ID: STD4=2.Oug/L
Seq. No.: 00007
A/S Pos.: —
Sample abs. is greater than that of the largest standard.
Replicate 1 Time: 13:56
=eak. Area (A-s): 1.762 Peak Height (A): 0.075
Date: 10/10/97 '
387
-------
.
Blank Corrected Pk Height (A): 0.075
Concentration (ug/L ' ): 2..100
Standard number 4 applied. [2.000]
Correlation 'coefficient: 0.99926 Slope: 0.0369
- Hg2 :. ID: STD5 = 5.0ug/L Seq. No.: 00008 A/S Pos. : — Date: 10/10/97
f Sample abs. is greater than that of the largest standard,
L_ Replicate 1 " Time: 13:57
Peak Area (A-s): 4.368 Peak Height (A): 0.187
i Blank Corrected Pk-Height '(A ): 0.187 .
Concentration (ug/L ): 5.063
f Standard number 5 applied. [5.000.]
I Correlation coefficient: 0.99989 Slope: 0.0372
\. -
• Ig2 ID: STD6=10.0ug/L Seq. No.: 00009 A/S Pos.: — Date: 10/10/97
I
w
Sample abs. is greater than that of the largest standard.
.' leplicate 1 Time: 13:59
' 3eak Area (A-s): 8.575 Peak Height (A): 0.378
'Blank Corrected Pk Height (A): 0.378
.Concentration (ug/L ): 10.154
Standard number 6 applied. [10.00O]
Correlation coefficient: 0.99994 Slope: 0.0377
388
-------
element File: HG_.MEL "- Element: Hg2
Date: 10/10/97 Time: 13:59
Data File: A8818.0AT ID/Wt File: A8S18.IDW
Technique: MHS Calib. Type: Linear
Remark 1: STANDARDS^ 3-020-7 . " -
Remark 2: QC= 3-020-8
Wavelength: 253.7 '
Slit: 0.7 L
Lamp Current: 0
Energy: 71 —r
H| Display Calibration - C:\fiflJSER\fifiJILES\ELEMEHT\HG_.MEL
Corp. Coef.: 0.99994
Slope; 8,8377
Concentration
1B.
'*.
.» '
•x
-------
.Element File: HG_.MEL
f 5ate: 10/10/97
LJata File: AB818.DAT
Teqbnique: MHS
("Remark 1: STANDARDS= 3-020-7
Remark 2: QC= 3-020-8
Element: Hg2
Time: 14:01
ID/Wt File: A8S13.IDW
Calib._Type: Linear
Wavelength: 253.7
Slit: 0.7 L
Lamp Current: 0
Energy: 71
f
ID: ICV=4.0ug/L
No
rReplicate 1 -
: 3eak Area (A-s): .3,624
' Jlank Corrected Pk Height (A): O.158
Concentration (ug/L- ): 4.204
00010 A/S Pos.: --
Time: 14:02
Peak Height (A): 0.158
Date: 10/10/97
Hg:
ID: ICB
Seq. No.: 00011
Replicate 1
"Peak Area (A-s): '0.023
alank Corrected Pk Height (A): 0.001
:oncentration (ug/L ): 0.035
A/S Pos.: —
Date: 1O/10/97
Time: 14:03
Peak Height (A): 0.001
! 192
ID: CHECK LO
Seq. No.: 00012
A/5 Pos.: --
Date: 10/10/97
Replicate L
;^eak Area (A-s): 0.188
1 ilank Corrected Pk Height (A): 0.008
Concentration (ug/L ): O.200
Time: 14:05
Peak Height (A): O.OOS
.92
ID: 43271 MB3
Seq. No.: 00013
• .eplicate 1
L eak Area (A-s): 0.000
Blank Corrected Pk Height (A): 0.000
Concentration (ug/L ): 0.000
A/S Pos.: --
Date: 10/10/97
Time: 14:10
Peak Height (A): 0.000
ID: 43271 MBS D
Seq. No.: 00014
.-^eplicate 1
Peak Area (A-s): 0.010
lank Corrected Pk Height (A): 0.000
oncentration (ug/L ): 0.008
A/S Pos.: --
Date: 10/10/9:
Time: 14:11
Peak Height (A): 0.000
ID: 43271 LCS3
Seq. No-.: 00015
A/S Pos.: --
Date: 10/10/97
eplicate
eak Area (A-s): 5.031
Wlank Corrected Pk Height (A): 0.234
Concentration (ug/L ): 6.198
Time; 14:12
Peak Height (A): 0.234
Hg2
ID: 43271 LCS3 D
Seq. No.: 00016
A/S Pos.: --
Date: 10/10/97
339
-------
Replicate 1
Peak Area (A-s~): 3.869
'Blank Corrected Pk-Height (A):
Concentration (ug/L ): 4.529
0.171
Time: 15:04
Peak Height (A): 0.171
Hg2 ID: CCV4=6.0ug/L
Seq. No.: 00061
Replicate 1
Peak Area (A.-s): 4.236
Blank Corrected Pk Height (A): 0.189
Concentration (ug/L ): 5.024
A/S Pos.
Date: 10/10/97^
Time: 15:06
Peak Height
(A): 0.189
Hg2
ID: CC84
Seq. No.: 00062 A/S Pos.: -- Date: 10/10/97
Replicate 1
Peak Area (A-s): 0.011
Blank Corrected Pk Height (A): 0.001
Concentration (ug/L ): 0.019
Time: 15:07
Peak Height (A): O.OO1
Hg2
ID: 183-43-11AB
Seq. No.
Replicate 1
Peak Area (A-s): -0.004
Blank Corrected Pk Height (A): 0,000
Concentration (ug/L ): 0.000
0006:
A/S Pos.: -- Date: 10/10/97,
Time: 15:03
Peak Height (A): O.OOO
Hg;
ID: 133-43-11AB D
Seq. No.: 00064
Replicate 1
Peak Area (A-s): -0.004
Blank Corrected Pk Height (A): 0.001
Concentration (ug/L ): 0.016
A/S Pos.: --
Date: 10/10/97
Time: 15:11
Peak Height (A): 0.001
Hg2 ID: CCV5=6.0ug/L
Seq. No.: 00065
Replicate 1
Peak Area (A-s): 4.880 "'.*
Blank Corrected Pk Height (A): 0.208
Concentration (ug/L ): 5.527
A/S
Pos.
Date: 10/10/97
Time: 15:12
Peak Height (A): 0.208
Hg2
ID: CCB5
Seq. No.: 00066
Replicate 1
Peak Area (A-s): 0.007
Blank Corrected Pk Height (A):
Concentration (ug/L ): 0.011
0.000
A/S Pos.: --
Date: 10/10/97
Time: 15:12
Peak Height (A): O.OOO
Hg2 ID: 43231 MB$«*».v<
-------
'f
J .Concentration (ug/L ): -0,003
L
Hg
ID: 43251 MSJ D
1
Seq. No.: 00063
Peak Area (A-s): 0.000
8 1 a n'k Co r r ec ted P K Height ( A ) : 0, 000
Concentration (ug./L ): 0.000
A/3 Pos.: —
Time: 15:14
Peak Height (A): O.OOO
Date: 10/10/97
HQ;
ID: 43231 LCS$
Seq. No.: 00069
f Replicate 1
i Peak Area (A-s): 3..900
Blank Corrected Pk Height (A): O.172
C Concentration (ug/L ): 4.574
A/S Pos.: —
Time: 15:15
Peak Height (A): 0.172
Date: 10/10/97
Hg
ID: 43231 LCS$ D
Seq. No.: 00070
"Replicate 1
f Peak Area (A-s): 4.077
i Slank Corrected Pk Height (A): 0.1S5
- JoncentVation (ug/L ): 4.912
A/S Pos.: --
Time: 15:'16
Peak Height (A): 0.185
Date: 10/10/97
ID: 1S3-3-1BC
Seq. No,
00071
A/S Pos.: --
Date: 10/10/97
r?eplic3te i
I eak Area (A-s): 0.017
"Blank Corrected Pk Height (A;: 0.001
Concentration (ug/L ): 0.013
Time: 15:17
Peak Height (A): 0.001
Hg2
ID: 183-3-1BC D
3plicate 1
Peak Area (A-s): 0.002
Plank Corrected Pk Height-.,
( jncentration (ug/L ): 0.
Seq. No.: 00072
: O.OOO
A/S Pos.: —
Time: 15:18
Peak Height (A): O.OOO
Date: 10/10/97
ID: 183-3-1BC MS
Seq. No.: 00073
RepLicate 1
F; ,ak Area (A-s): 4.103
E_ ank Corrected Pk Height (A): 0.182
Concentration (ug/L ): 4.827
A/S Pos.: —
Time: 15:20
Peak Height (A): 0.132
Date: 10/10/97
Hg2
ID: 183-3-18C MSD
Seq. No.: 00074
R olicate 1
pLak Area (A-s): 3.914
31ank Corrected Pk^Height (A): 0.174
^l icentration (ug/L ): 4.619
A/S Pos,
Date: 10/1O/97
Time: 15:20
Peak Height (A): 0.174
-------
Hg2 ID: 183-3-5BC
Seq. No.: 00075
Replicate If.
Peak^Area (A-s): 0.007
Blank'Corrected Pk Height (A): 0.000
Concentration (ug/L ): 0.003
A/S Pos.: —
Time: 15:22
Peak Height (A-): 0.000
Date: "10/10/9"
ID: 183-3-5BC D
Seq. No.: 00076
Replicate 1
Peak Area ('A-s): 0.002
Blank Corrected Pk Height (A): 0.000
Concentration (ug/L ): 0.005
A/S Pos.: --
Time: 15:22
Peak Height tA): 0.000
Date: 10/10/S
Hg2
ID: CCV6=6.0ug/L
Sea. No.: 00077
A/S Pos.: --
Date: 10/10/97
Replicate 1
Peak Area (A-s): 5.364
Blank Corrected Pk Height (A): 0.232
Concentration (ug/L ): 6.150
Time: 15:23
Peak Height (A): 0.232
ID: CCB6
Sec
No.
0007S
A/S Pos.: --
Date: 10/1O/O
Replicate 1
Peak Area (A-s): 0.009
Blank Corrected Pk Height (A): 0.000
Concentration (ug/L ): O.OOS
Time: 15:25
Peak Height (A): 0.000
r 1
392
-------
TECHNICAL REPORT DATA
Please read instructions on the reverse before completing
1. REPORT NO.
EPA-454/R-99-017A
2.
4. TITLE AND SUBTITLE
Final Report - Iron and Steel Foundries Manual Emissions Testing of Cupola Baghouse at
Waupaca Foundry in Tell City, Indiana
Volume I of II
7. AUTHOR(S)
Franklin Meadows
Daniel F. Scheffel
9. PERFORMING ORGANIZATION NAME AND ADDRESS
Pacific Environmental Services, Inc.
Post Office Box 12077
Research Triangle Park, North Carolina 27709-2077
12. SPONSORING AGENCY NAME AND ADDRESS
U.S. Environmental Protection Agency
Office of Air Quality Planning and Standards
Emissions, Monitoring and Analysis Division
Research Triangle Park, North Carolina 2771 1
3. RECIPIENT'S ACCESSION NO.
5. REPORT DATE
June 1999
6. PERFORMING ORGANIZATION CODE
8. PERFORMING ORGANIZATION REPORT NO.
10. PROGRAM ELEMENT NO.
11. CONTRACT/GRANT NO.
68-D-70069
13. TYPE OF REPORT AND PERIOD COVERED
Final
14. SPONSORING AGENCY CODE
15. SUPPLEMENTARY NOTES
16. ABSTRACT
The United States Environmental Protection Agency (EPA) is investigating iron and steel foundries to identify and quantify hazardous air pollutants
(HAPs) emitted from cupolas; electric arc furnaces; and pouring, cooling and shakedown operations of sand mold casting processes. The Waupaca
Foundry in Tell City, Indiana was selected by the EPA as the host facility at which to 1) characterize HAP emissions from cupolas that are controlled by
baghouses, and 2) assess baghouse performance in controlling HAP emissions from cupolas. The Waupaca Foundry was selected because EPA
deemed this facility to be representative of a large segment of the sand casting foundry industry. Waupaca Foundry operates a large cupola (SO standard
tons per hour melting capacity) that is controlled by a negative pressure baghouse. The new facility recently began production and the modern design of
the cupola baghouse was expected to be as effective as any used in this type of application.
This report presents the results of a manual emissions testing program to characterize emissions from a cupola and assess the performance of the
baghouse in controlling HAP emissions. Testing was conducted at the cupola baghouse inlet and outlet to determine air emissions of particulate
matter (PM) and metal HAPs; and at the cupola baghouse outlet to determine organic HAPs consisting of dibenzo-p-dioxins and polychlorinated
dibenzodurans (PCDDs/PCDFs), and semi-volatile organic hazardous air pollutnats (SVOHAPs). The data may be used by the EPA as potential
Maximum Achievable Control Technology (MACT) floor technology for cupolas.
During the testing program, Research Triangle Institute (RTI), another EPA contractor, monitored and recorded process and emission control system
operating parameters, and prepared Section 3.0, Process and Control Equipment operation, of this report.
This volume (Volume I) is comprised of 569 pages and consists of the report text, and Appendices: A (Raw field Data), and B (Analytical Data -
Particulate Matter and Metals).
1 7. KEY WORDS AND DOCUMENT ANALYSIS
a. DESCRIPTIONS
Baghouse
Cupola
Dioxins/Furans
Emission Measurements
Hazardous Air Pollutants
Metals
Particulate Matter
Semi-volatile Organic Hazardous
Pollutants
18. DISTRIBUTION STATEMENT
Unlimited
b. IDENTIFIERS/OPEN ENDED TERMS
I
19. SECURITY CLASS (This Report)
Unclassified
20. SECURITY CLASS (This page)
Unclassified
c. COASTI Field/Group
21. NO. OF PAGES
1,066
22. PRICE
-------