M1V-? X3tS*'~- •*
                                                                        FBS6-216470

                                                                         C t- ^> i
          Unitec3  States  Procedures for Sampling  and
          Analysis  of.  Hasardouo Waste
          Systems,  Science and Software, San  Diego,-
                                               CA
          Prepared  £or


          Environmental Protection Agency,  Cincinnati, OH
          Jul  86
     L
                                                    Jy^^S3 J JA.'-~
U.S.
                  3 ©J
          «00/D
          86-128
          Copy 2
          BWC
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                                                             ENVI vJO^r laN'v
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                                                                 2@IO;3 0

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                                                                                     PB86-216470
                                                                       EPA/600/D-86/123
                                                                       July  1986
                  UNITED STATES PROCEDURES FOR SAMPLING AND ANALYSIS  OF  HAZARDOUS WASTE


                                                    by
                                               Eugene Burns
                                        Systems, Science & Software
                                         San Diego, CA 92121-1095
                                           EPA Project  Officer
                                               Clyde  J.  Dial
                             HAZARDOUS WASTE ENGINEERING  RESEARCH LABORATORY
                                    OFFICE OF RESEARCH AXD  DEVELOPMENT
                                   U.S. ENVIRONMENTAL PR01ECTION AGENCY
                                          CINCINNATI, OH  45263
                                          KPSODIJCfO B»
                                          NATIONAL TECHNICAL
\                                         INFORMATION SERVICE
                                             (I.S. DEP*»W»: OF COMMERCE
                                               SPRIHGflflB, »». 22161

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«. A J —^' —
                                                TECHNICAL RK?OHT DATA
                                         (Pleau read Instructions on the reverse he fore corr.ple.ing/
            1. FEPORT NO.
              EPA/600/D-36/128
             3. RECIPIENT'S ACCESSION WDf"H If.?
              PE3 6   >> 1  {->  - < U /ftS
            a. TITLE ANDSUBTITLE
              United States  Procedures for  Sampling and
              Analysis of Hazardous Waste
                                                                         5. REPORT DATE
                                                                             July  1936
             6. PERFORMING ORGANIZATION COOS
            7. ALITHOR1S)
              Eugene Burns
                                                                         8. PERFORMING ORGANIZATION REPORT NO.
            B. PERFORMING ORGANIZATION NAME AND ADDRESS
              Systems, Science & Software
              3398 Carmel Mt.  Rd
              San Diego, CA 92121-1095
            12 SPONSPRING AG6NCV NAME ANO ADnacCC
             Hazardous Waste Engineering ;\esearch  Laboratory
             Office of Research and Development
             I'.S.  Environmental Protection Agency
             Cincinnati , OH  452f>8
                                                                          10. PROGRAM ELEMENT NO.
             11. CONTRACT/GRANT NO.
                                                                          13. TYPE OF REPORT AND PERIOD COVERED
             14 SPONSORING AGENCY CODE

                 EPA/600/12
            15. SUPPLEMENTARY NOTES
            16. ABSTRACT
              This naper WAS  prepared  for presentation  at a joint  US/Spain Seminar on /-:/ardous
              Waste Management, to be held in Madrid,  Spain, on May 19-22, 1936.
              Topics include  identifying  hazardous  compounds, sampling methods,  analysis
              methods and  quality assurance approaches/procedures.
                                             KCY WORDS AND DOCUMENT ANALYSIS
                               DESCRIPTORS
            18. DISTRIBUTION STATEMENT
                RELEASE  TO PUBLIC
                                                            b.lDENTIFIERS/OPEN ENDED TERMS  C.  COS* Tl Field/Group
19. SECURITY CLASS ITha Keport/
  Unclassified
                                                            20. SECURITY CLASS (Tha pagt)
                                                               Unclassified
21. NO. OF PAGES
      112
                                                                                        22. PRICE .
            EPA Form 2230-1 (R«r. 4-77)   PRCVIOUS EDITION IS O«IOLEie -•

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;
                                                            NOTICE





                            This  document  has  been  reviewed  in  accordance with  the  U.  S.  Environmental



                        protection Agency  policy and  approved for publication   Mention  of trade  names



                        or  commercial  products does not  constitute  endorsement  or  recommendation  for



                        use.
                                                               11

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                                    FOREWORD


     Tooay's rapidly developing and changing technologies and industrial

products and practices frequently carry with them the increased generation

of solid and hazardous wastes.  These materials, if improperly dealt with,

can threaten both public health and the environment.  Abandoned waste sites

and accidental  releases of toxic and hazardous substances to the environment

also have important environmental and public health Implications.   The

Hazardous Waste Engineering Research Laboratory assists ;n providing an

authoritative and defensible engineering basis for assessing and solving

these problems.  Its products support the policies, programs and regulations

of the Environmental Protection Agency, the permitting and other responsi-

bilities of State end local governments and the needs of both large and small

businesses in handling their wastes responsibly and economically.

     This report identifies hazardous compounds, sampling and analytical

methods for measuring these compounds, and procedures that can be used to

assure the quality of data obtained.  This report should be useful  to those

who are faced with assessing the extent of hazardous compounds or determining

the efficiency of control approaches.

     For further information, please contact the Alternative Technologies

Division of the Hazardous Waste .Engineering Research Laboratory.
                                       David G. Stephen, Director
                           Hazardous Waste Engineer! ny Research Laboratory
                                      iii


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•                                                  ABSTRACT


I                     '    .
ji

^                   Hazardous waste may oe stored, treated and disposed in i.  variety of
i!


[            •  ways.  Treatment technology exists today for detoxification or destruction

ft

-f              of wastes in an environmentally acceptable manner through physical, chemical

V

'              and biological means.  This paper identifies hazardous compounds, sampling



              and analytical methods for measuring these compounds, and procedures that



'              can be used to assure the quality of dat? obtained.  This report should be



|              useful to those who are faced with assessing the extent of hazardous compounds



:              or determining the efficiency of control approaches.
                                                     1v

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                                                  CONTENTS
i

              Foreword	  .  .  lii

              Abstract	  iv

              Tables 	  .............  vi

              Figures	vii

."              SECTION 1                                                                    1
Li
i                 Introduction	   I

:              SECTION ?

[                 Scope--! Jenti fied Hazardous Compounds .......'...	   5
t
\              SECTION 3                                                                    8

I,                 Sampling Methods	   8

|                 Sol-.ds	   9

|                 Liquids	:	13

i                 Gases   .	16

I              SECTION 4       '                                                        '21

                 Analysis Methods  	  24

                 Survey Analysis	30

                 Sample Preparation Procedures  ......	  .  33

                 Organic Constituents   	  34

                 Inorganic Constituents	•.	38

                 Organic Analysis Methods   	 .  	  39

                 Monitoring	42

                 Inorganic Constituents   	  43

              SECTION 5                                                     .48

                 Quality Assurance ana  Qua^ty  Control Procedures	48

              REFERENCES                                                   '               56

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rtr
                                                      TABLES
                                                                                            Page
                 Table  1.

                 Table  2.

                 Table  3.

                 Table  4.

                 Table  5.

                 Table  5.


                 Table  7.

                 Table  3.

                 Table  9.

                 Table  10.

                 Table  11.

                 Table  A.I
Source Lists for ITD/RCP.A Analytes  .  .

Choice of Samplers for Hazardous Waste

Sampling Points   	.  .  .  .  .
                                                                   6

                                                                  10

                                                                  11
Sampling Methods for Effluent Streams ........  	    12
Waste Evaluation Procedures
                                                                  25
Threshold Levels of Contaminants in the
  Extraction Procedure Toxicity Test  .
                                        	    28

Proximate Analysis of Wastes  	  	    31

Sample Preparation Procedures 	  .  .  	    35

Routine/Monitoring Organic Analytical  Methods  .........    44

RCRA Methods for Metal  Analysis of Wastes	  .    46

Essential Flements of a QA Project Plan   	    49

ITD/RCP.A Compound Data	  59 -  104
                                                        v1

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                                    FIGURES



                                                                       Page
                                                                       -..---**

Figure 1.   Modified Method 5 Train (HM5)  . .  .,	      2:0

Figure 2.   Volatile Organic Sampling Train (VOST)   	      23

Figure 3.   Diagram of a sampling and analysis  procedure whicn
           uses replicate samples to provide  information on
           sources of variance	      54
                                       vii

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                                                   SECTION 1
                                                 INTRODUCTION






(                   Under  the  Resource  Conservation and  Recovery  Act  (RC8A),  the  United
i

i              States  Environmental   Protection  Agency   (EPA)   has   promulgated  proposed,


1              interim,  and   final   regulations  for  owners/operators  of  hazardous  waste


;              treatment,  storage and  disposal  facilities (TSOFs)  These  regulations  state

i                                       '               .

'•              that generators  of  hazardous waste are responsible  frcra "cradle to grave" for

t

;              these   materials.    Additionally,   under   the   Comprehensive   Environmental
s

\              Response,  Compensation  and  Liability  Act   (CERCLA), the EPA has  promulgated


f              regulations  which   govern  the  cleanup  of   hazardous  wastes  at abandoned  or


]              uncontrolled disposal  sites.  Tnis law antS  the associated regulations provide


;              legal mechanisms for  (1) assessing actual or threatened releases of hazardous


               substances  at  uncontrolled  sites,  (2)  implementing clean-up activities,  and

j
\              (3)  recovering  cleanup  and  resource  restoration  costs  from  the  parties


?              responsible for the hazardous wastes.
                    Key to the  identification  of  a hazardous waste site or hazardous waste is
 *
 i
 j
 i

 i


 !               the confirmation that specific  chemical  species which have br.en  listed  by EPA
 i

 I               as hazardous are  present (Ref,  1-4).  This  is determined by  (1)  prior cxperi-

 i   '
 j               ence of the  operator/owner in  knowinq what  is present  
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     Specifically, these  strategies  roust be  designed  to ensure that  the data
generated  meets  the  quality requirements  and  intended  purpose of tie  waste
characterization   effort.    If   a  measurement   activity   is  performed   in
conjunction  with   a  hazardous   waste  permit  prog"am,   for   example.  &V\
information  needed   to  establish  compliance   should  t>e   generated.    As  a
consequence,  the  wast<»  characterization  strategies  may vary  significantly,
depending upon the Intended use of the information.

     Clearly,  the  waste cfu racterizatlon  strategy will  include consideration
of  sairpling  procedures  and  the  selection  of  suitable  chemical  analysis
procedures,   together   with   Information    regarding   sample   preservation,
packaging, storage and shipping  to the  analysis  laboratory.   The strategy will
also.  Include  a   procedure  to   ensure  that ,. an  effective  chain-of-custody
procedure  is  incorporated  Into the   saspllng  protocol.    Other  important
considerations  Include  the  sarnie  size  to  be  collected  (e.g.,  sufficient
sample  roust  be   obtained   1n   order   to   make   measurements   In   the  need-z.s
concentratlon  range).   The .sampling  protocol  will  also  contain  explicit
provisions for ensuring  the  safety of the  personnel  collecting  tha samples at
the sampling site.

     The  collected  raw  or  treated  waste  will  be  evaluated  using  a set  of
regulation-specified  physical and  chemical  tests  to  determine  whether  1t insets
the definition of  a  hazardous  waste.    The  owner/operator  of  the  hazardous
waste treatment, storage, and disposal  facility  (TSDF) first determines  1f his

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rr .7.  „'_"._   "~. r	~'  '  ~""'
               waste  1s excluded .1n  Section 261.4 cr  specifically  listed  under Subpart D of
               the  RCRA regulation.   If the waste  ii  not  excluded  and not  listed,  then he
               must  evaluate  his  waste  1n  terms of  four  hazardous  characteristics:   ignit-
               sbillty.  corrrsivity,  reactivity, and  EP  Toxldty,   unless  he  can  property
               evaluate  the  waste based  on his own knowledge of the waste.

                   The  definition of  hazardous taste  specified 1n  40 CFR  261.1  for toxic
               constituents  In the  extraction  procedure are  IR  the  process  of expansion to
               cover  a wide  range  of generally  recognized toxic Inorganic  end oroanic com-
               pounds  and  nnstures.   For hazardous waste Incineration processes, for example,
               clear-cat   regulations  requiring  the destruction of  99.99*  percent  of  the
               principal  hazardous  constituent  have been  defined  1n 40 CFR  264 (f'enaitting
               Stanoirts]  and 40 CFR 2f>5 (Interim Status  Standards).   !P sany  cases, defini-
               tive  analytical- sathods and  regulatory  concentration  levels  have not  yet been
               established and each waste is considered on  a case-by-case basis.

                   The  objective of  this   paper is  to provide a managenvent  overview  of  the
               current status of  procedures  used in  the United States for sampling the  myriad
               of  hazardous   waste  form and for  obtaining maaningful concentration measure-
               ments  at trace and macro levels  of identified hazardous compounds in the waste
               nutrix.   Detailed and  generalized discussions  of these  rstethods  are presented
               1n  References  1-4.    This paper  presents  discussions on  sores  specific  and
               generalized  analytical   Bsethods  which   are  currently   used  and  descriees
               promising   analytical   techniques   directed  toward   cofspounds   for   which

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non-validated  methods  exist.   Finally,  Information  is  provided  on  quality
assurance  and  quality  control  procedures which  are  required  to ensure  that
data  generated  are  complete,  representative,   comparable,  valid,  of  known
precision and accuracy, and legally defensible.

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f
\
[                                                  SECTION 2
                                     SCOPE  -  IDENTIFIED  HAZARDOUS  COMPOUNDS





                     Since  1971,  the United States  EPA  has  been Identifying specific  chemical


                compounds which are considered environmentally toxic.  As a result of  the  1976


                Consent  Decree, a comprehensive list of toxic water  pollutants was generated  -


                the  priority  pollutant list.   In the intervening years, it has been determined


                th?t  additional compounds and  classes of compounds  also provide a  toxic concern


                and  need to be added  to  the list of  hazardous  materials.  Presented as an appen-


                dix  to this  paper  is the most  recent  list;  namely,  the Industrial Technology


                Division/Resource  Conservation Recovery Act  (ITD/RCRA)  list which defines the


                compounds to  be  analyzed in  the ITO/RCRA  Sewage Study project (Ref. 5).   This


                list  includes all  compounds   on  the RCRA Appendix VIII  list  (40 CFR 261.33,


                Appendix  VIII),  the  proposed  addition  to that  list  (Michigan Petition,  49 FR


                49793.  21  December  1984),  the  priority  pollutants, the  Super-fund compounds


                (Hazardous  Substance  List)  the  Paragraph 4C and Appendix  C  compounds,  and


                additional  specific  compounds which are  part of  the  class  or  group  of  com-


                pounds  entered  on one of the  above  lists.  There are a total of  676 compounds


                or classes of  compounds  on   this  list,  with considerable overlap  among the


                source  lists. Table  1   lists  the  number of compounds  or classes of compounds


                Identified  in each of the  source listings. The  compounds  on the source lists


                total 946,  but when  redundancies  are eliminated, the  total is 676.





                     The  ITO/RCRA  "list of  lists*  shown in  the  Appendix  contains empirical


                formulas  for the  compounds,   when  possible,   chemical  abstract  system ('CAS")


                registry  numbers,  and other unique  identifying  numbers  when  no CMS number has


                                                       5

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been  assigned,  an  indication of  the  type  of analysis  that  is  known or  is
probably  applicable,  the  promulgated  EPA  method,  when  there  is  one.   and
reference  to  a RCRA method, when  applicable.   Identification  of new and/or
modified  analytical   methods is  under  way,  and  this  information  is  being
updated as methods are validated.


                  TABLE 1.   SOURCE LISTS FOR ITO/RCEA ANALYTES

         Source List              Number of Compounds        ITD/RCRA List

     RCRA Appendix VIII                  427
     Hazardous Substance List            128
     Priority Pollutant List             154
     Michigan Petition                •   121
     Paragraph 4C                         56
     Appendix C                           23
     Sewage                               37
            TOTAL                        946
676
     The  ITD/RC8A list  of 676  compounds  is  clearly  the most  comprehensive
listing  of  regulatory-Identified hazardous  compounds  or  classes  of  compounds
assembled to  date.   An  objective  of the  ITD/RCRA  Sewage  Study project  is  to
Identify  and   validate  sampling  and  analytical methods  which  would  permit
quantitation  of  these  pollutants  in  either  trace  or   macro  quantities  in
hazardous  wastes.   It  should  also  be  recognized  that  several  of  the  676
compounds  hydrolyze  or  react  with  water,  which   if present  in  the  waste

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                                    SECTION  3

                                SAMPLING METHODS

     The sampling methods  which  are required for the  ultimate  analysis  of the
ITD/RCRA list of  compounds in hazardous waste must  be applicable  to a veriety
of media and waste  forms.   Hazardous waste  forms  may be solid,  liquid, slurry,
or sludge.  Hazardous  waste from effluent process streams  may  also be gaseous
or particulste-laden  gases,  and  in this  context particulate  matter includes
discrete particles from both solids and liquid aerosols.

     The essential  part of any sampling  method  1s  to assure that  a sample is
acquired which  Is  representative  of  the  waste that  is being  analyzed.   The
analytical result 1s only  as  good  as the  sample which has been collected.   For
waste  thet  contains two  phases,  and  ones that  contain particles  of varying
sizes, it is essential  that a  maans for making  such  a heterogeneous mixture as
close to homogeneous as possible be employed.   A  means for agitating the waste
1s useful to  ensure that a representative  sample is acquired.   Alternatively,
1f discrete phase.layers  exist within a  sample,  it  1s also possible to  obtain
a representative  sample frora  each  layer  and  then by  determining  the relative
volume and/or weight of the layer within the waste,  a calculated  value  of the
chemical constituents  1ri the  combined separated waste  can be made.  In  most
cases, an  easier prospect  is  to  use  the prior  approach  of mixing  a hetero-
geneous mixture  and collecting  as representative a  sample as  possible.   For

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complicates their analysis.  A classic example.>s  the  case of bis-chloromethyl
ether, which  has a  half-life in  water  of  seconds.  Because  of  the  !?ck  of
validated methods for  many of  the ITD/RCRA compounds, those  compounds  are not
now being used for regulatory purposes.   The  "11st of  lists"  is presented here
because it shows the direction to which the EPA 1s moving.
                                        .^

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                           TABLE 2.  CHOICE OF SAFJ'IERS FOR 5SAZARDOUS  WASTE

         Waste Type

Liquids, sludges  and slurries.
in drums,  vacuum trucks, bar-
rels, and similar containters
Liquids end  sludges  In ponds,
pits or 1639003
Wastes in storage tanks
Dry  wastes  (in  shallow con-
tainers) and sjrface soil

Waste piles
Source - Reference 2
                                   (b) Class
(o) Dipper
                                   (b) Weighted Bottle
Weighted BHtlo
Powdered or granular solids  in    (a) Tliiof
bags, drums or containers
(b) Trisr


Trowel


Wasto Pile Sampler
             L i a i to t ions/CommonIs

Nat tor containers X.&ia deep.

Hot for Bastes conjoining ketonus, nitrobenzene,
dioethylformamide, aoaityl oxide, or t.etrahydro-
furan.

Mot for oastss  containing hydrofluoric acid and
concentrated alfciiii solutions.

Cannot be used to  collect samples beyond 3.5m;
dip  and  rotriov:-   eapplor  sioojy  to  avoid
bending tho t~.ti'.;;«r aluoinua handle.

May be difficult to uso on viscous liquids; the
bottle  may  also   bo   used   83  Uio  samp Io
container.

Uay be difficult to  use on viscous liquids; the
bolt Id day also bo used as tho sample container.

Liaitod  application  for   sampling  ncist  and
sticky  no I ids  end  when  the  diameter  of thr>
oolids is greater than 0.6 era.

Uay incur difficulty in  retaining a core sample
of very dry granular materials during sampling.

Nob applicable  to  sampling  cloopor  than 8 cm.
Difficult to obtain c reproducible samplo mass.

Hot applicable  to  sampling  solid  castes nith
dimansions greater than one-half the diameter of
the sampling tube.

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effluent  streams  that  have good  points  of  mixing within  the  pipeline,  the
collected  proportional   sample  is  a  ready  means  for  sample  collection  and
assumes a homogeneous mixtures has been acquired.

     The preferred method  for  sampling hazardous waste  depends upon  the exact
form of the  waste.   Table 2 presents  a  summary  description  of  general  methods
which are to  be  used for the sampling of  hazardous  waste.   Table 2 summarizes
the sampling devices appropriate  for the hazardous  waste sampling,  and  Table 3
summarizes sampling  locations  .'or most  waste containers.  Table 4 identifies
preferred methods  for  sampling effluent waste  streams as a  function of waste
type.
SOLIDS
     A wide  variety  of sampling  tools  and  equipment are  available for  the
sampling  of  solid  materials.   The  methods most  used for  sampling of  solid
hazardous waste  are  the sample corer  (trier),  the grain  sampler  (thief),  and
the trowel, scoop or shovel.

     The  trier  or  sample  corer  consists  of  a  long tuba  with  a  slot  that
extends  nearly the  entire  length  of   the  tube.   The waste  pile  sampler  Is
essentially a  large  sample corer.  These samplers  are easily  fabricated  from
sheet matal  or plastic  (PVC)  pipe.   The Up  ani  edgas  of  the tute slot  are
sharpened  to  allow  the  corer to  cut  a  core  of material to  be  sampled  when
rotated  after  insertion  into the material.  The sampler   is inserted into  the

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               CONTAINER

bruit (bung on one ond)

Drum (bung on side)
                                       TABLE  3.   SAMPLING POINTS
                       SAMPLING POIHf

.Withdraw sauplo through the bung oponing.

Lay druir. on side  eith  bung  up;  BiUidra
bung
Barrels, fiberdrums,  buckets, sacks, or
bags
Vacuum truck (or sienilar)

Ponds, pits, lagoons




Waste piles



Storage tanks

Soi Is
                                            sample through the
Withdraw  samples  through  the  top  uf  Ijarrols,  fiberdrums,
buckets, ond ,»irailar containers,  or  through Hi)  openings of
bags and sucks;  aithdrao  sample  through  t!i(j  contsr of the
containers and  to  different  point?  diagonally opposite the
point of entry.

Hithdraa sample through open hatch; maple nil other hat.hcs.

Divide  surface  oroo  into  an  Imaginary  grid;*   take three
samples, if possible:  one  sample near surface, one sample at
mid-depth or at center, and  one  sample at the bottom; repeat
the sampling at each grid over tho ontiro pond or site.
         subsurface sairple  through  at  least three different
points near the top of  pile to points diagonally opposite the
point of entry.

Withdraw cample from the top through the sampling hole.

Divide the surface area  into  an Imaginary grid;« sample each
grid.
«llie number of grids is determined by the desired  nurr.ber of samples to be collected ohich, nhen combined,
will give a representative sample of tho naste.


Source - Reference 2

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                 TABLE 4.   SAMPLING METHODS FOR EFFLUENT STREAMS
        Waste Type                             Methods
   Solids                      Scoops, Trowels
   Liquids                     Proportional Samplers, Tap Sampler
   Sases                       Gas Bulbs, Sas Bag Sampling, Fence line Monitors
   Slurries                    Dippers, Tap Samplers
   Particulate*-Laden Gases    Stack Gas Methods:
                                  Hodified Method 5 (MM5)
                                  Source Assessment Sampling Systems (T.ASS). or
                                  Volatr.e Organic Sampling Train (VOST)

   *Includes solids and liquid aerosols.
waste at  an oblique angle  to  a depth established by the  sampling  protocol  to
ensure  statistical- representation.   The sampler 1s  rotated  and  then withdrawn
with  the  open  portion  of the  trier  pointed  upwards.    The  trier  1»  the
preferred method  whcri  powdered or  granulated  material  to be  sampled  is  moist
or  sticky.   At any case,  to  ensure homogeneity  for  solid  samples, cone  and
quartering  procedures  are employed to  reduce  the total solid waste collected
dcwn to a size manageable for analytical measurements.

     Alternatively, an auger can be used  to obtain samples.  It 1i  particularly
useful  for  hard or packed solid waste or soil.  An auger consists  of sharpened
spiral  blades  attached to  a  hard   metal  central  shaft.   To obtain  samples  at
specified depths  within  i waste sample, 1t  is  usually  necessary to drill down
                                       12

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                 to a  specified  d-ipth  and  either isolate or discard the waste for the depths of
                 no interest and then  proceed  to use the auger for the desired additional depth
                 of the sample.

                      The  grain sampler,   also  called  a  thief,  consists  of  two  slotted
                 telescoping tubes,  usually made  of  brass or  stainless  steel.   The outer tube
                 has  a conical  pointed  tip on one end, which  permits  the sampler to penetrate
                 the  rtaterfal  being  sampled.  The sampler  is  opened  and  closed by rotating the
                 inner tube.   While  open,  the  sampler is shaken to pernit a free-flowing sample
                 to  fill  the   interior  of the  sampler.   The  grain  samp'ler  is   useful  for
                 obtaining  multiple  samples   at  different  depths  within  the  free-flowing
                 hazardous waste sample.

                      The trowel. scoop  and shovel procedures  are often used to acquire samples
                 from conveyor belts.   The  laboratory  scoop is similar to a trowel, except the
                 blade  on  the trowel  is more  curved and  has  a closed upper lip to permit thf.
                 containment  of  the material.  An  ordinary  zinc-plated  garden  trowel  can oe
                 used  in some cases to  sample  dry,  granular  or powdered materials  in  bins or
                 other  shallow  containers.  Tha laboratory scoop, however,  is a better device
                 because  it  Is  usually  reade of  materials  less subject to corrosion  or chemical
                 rsactions, thus minimizing sample contamination.

                 LIQUIDS

                       Liquid   samplers  that are  most  used for  hazardous  wastes  include  the
                 Coliwana, a weighted  bottle (thief), a  dipper, or  pond sampler and a tap.
                                                         13
L

                                                                                                    ,

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     The  Coliwasa  is  a  device  employed  to  sample  free-flowing  liquids  and
slurries  contained  in  drums,   shallow  open-top  tanks,  lagoons,  pits,  and
similar containers.   It is  especially usefu1  for sampling waste that  consists
of  several  immiscible  liquid  phases.   The  Coliwasa  consists  of  a  glass,
plastic,  or  matal  tube  equipped  with  an  end closure  that  can be  opened  and
closed  while  the tube  is submerged  in  the material  to be  sampled.   Coliwasa
samples  can   be  collected  rapidly,  thus  minimizing  exposure of  the  sample
collector  to  the potential  hazards of  the waste.   In  addition,  the  Coliwasa
sampler is simple  to fabricate  and inexpensive enough  that  contaminated  parts
can be discarded after  a  single  use if the parts  cannot be cleaned easily.  The
selection of the sampling tube material  (PVC  or porosilicate glass tubing)  for
particular waste 1s determinc-d by the components of the waste (see  Table 2).
                          fc
     To. collect  the  waste sample,  open the sampler by piacing the stopper  rod
handle, push  the rod down until  the  handle sits against the sampler's locking
block.  Slowly  lower the sampler  into  the waste  at a  rate  that equalizes  the
level of  liquids cutside  and  inside the .sampler.   If  the level of  waste in  the
sampler is lower inside than outside, the sampling rate would be  too  fast  and
will  produce  a  non-representative  sample.   When  the  sampler Is  submerged to
the desired  depth  or hits the bottom of the waste cylinder,  push  the sampler
tube down  to  close and lock the stopper by turning tha  *T"  handle until  it 1s
upright and  one end  rests  on the locking block.  The Coliwasa  1s  withdrawn
from the waste and wiped  dry  with  a disposable  cloth  or rag.  The  waste sample
is  transferred  to  a  storage container and  the  process  is  repeated   until  a
                                       14

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                requisite  quantity  of  sample  has been  collected.   The  use  of Coliwasa  is
                limited to sample  depths  less than 1.5 meters.   However,  this  is adequate for
                waste containers, shallow lagoons, and drums, barrels, or tanks.

                     The  weighted  bottle  sampler consists  of  a  glass  or  plastic  bottle,
                sinker, stopper  and a line that, .is used  to lower,  raise  and open  the bottle.
                The  weighted bottle samples  liquid   and free-flowing  slurries from samples
                contained in storage  tanks, wells,  sumps, and  other containers  which cannot be
                sampled adequately  with  other  liquid sampling  devices.   To acquire  a- liquid
                sample  using a  weighted  bottle,  the bottle  is  lowered  to  the  appropriate
                depth, uncapped, and  after  completely filled the sample is withdrawn. Once out
                of the  waste,  the bottle 1s  capped,  rinsed off, and  used as a sample storage
                container.   The  sampler  cannot  be  used  to  collect  liquids  that  are  Incom-
                patible with or chemically reset with the weight sinker or the control lines.

                     The dipper  ojr  pond sampler consists of a  glass or plastic beaker clamped
                to the  end  of  a two-  or three-piece telescopic  aluminum or  fiberglass  pole
                (which  serves  as  a  handle).  The   dipper  samples  liquids  and  free-flowing
                slurries from ponds,  pits,  tanks  with open tops,  and lagoons.   Dipper samples
                are  collected  from  open  streams  such as  sluices, or  from  open tanks  where
                there is  sufficient access  to permit  the  insertion and removal of  the dipper.
                The sample 1s collected by  Inverting  the  beaker and Insertion of the pole into
                the waste liquid or slurry  at an  oblique  angle.  At the appropriate depth, the
                beaker  is  turned right-side  up and   allowed  to  fill  completely, as evidenced
                by the  cessation of air  bubbles  at the  top surface of  the waste.   The  dipper
                is raised and the sample  is transferred to an appropriate storage container.
                                                       15
i.-i.-i a^..

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     Tap  sampling  is  the appropriate  method  for  sampling  liquid  wastes  in
static  or effluent pipes  or ducts.  Coliwasa  sampling  is not  appropriate  to
the collection of  liquids  from moving streams.   For liquids  in motion,  such  as
Industrial discharges  or  scrubber waste mixtures, a tap either  in  the  process
line  or  in  the  storage  reservoir permits  acquisition  of  a  representative
sample.   Commercial  proportional  samplers  are  often  used to  open and  close
valves periodically and provide  a  time-aversged  sample.  In  this method,  a tap
1s attached  to the waste  stream line and a  portion  of  the  flowing  liquid  is
diverted  Into  a  sampling bottle.  When  sampling  non-volatile liquid  products,
the sampling apparatus  should  be filled and  allowed to  drain before  acquiring
the actual  sample.   If  the  actual  sample   1s  to  be  transferred  to  another
container, the  sample container should  be  rinsert with sorae  of  the product  to
be sailed and drained before  it  is filled with  the actual  sample.   A  propor-
tional saucer usually provides this rinsing ooeration  automatically.
GASES
     Hazardous waste gases are collected  by  a  variety  of  techniques,  depending
if they  are from a  static  or flowing  source.   For static gases,  it  is  first
necessary to  know the pressure within  the container.   Hazardous  /ilgh-pressure
gas under  static  conditions is sampled by  allowing the gas to blow  down  into
either an evacuated vessel or a gas bag sampling system.

     For gas  bulb sampling, a glass  bulb is evacuated prior to  connection  to
the sample  line.  The  gas bulb  is  connected  to the a valve on  the container  to
be sampled, and usually  the  volume  between  the tank valve and  the gas sampling
                                       16

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                   valve  1s  evacuated.   The  gas storage  tank valve  Is  opened and  then the gas
                   sampling  bulb  valve  is  carefully  cracked  open  and  allowed  to  fill  to
                   approximately  1 atra.   A rsanon^ter 1s used  to  ensure that this pressure Is not
                   exceeded.   If  a   corrosive   gas  1s  sampled,   the  pressure fssasuring  device
                   contact  surface  must be  cheia'.cally cofspat'ib'e with  the  toxic  gas.   It is
                   Important  to not  let the  glass bulb  pressure excsect  1  ats when  siting a
                   high-pressure gas  source  oecause the  high pressure could fracture the glass, or
                   blow out the valve  stopcocks  and hence  lose the  sample.
                        For   Tow-pressure   hj>--rdous  gas   s.'rsples   (less  than  one
                   pressure),  tne  evacuated  bulb  1s  connected  to  the  vessel  and  the  volume
                   between the  two  valves  1s evacuated.   Then tha tank 1'» opened -incs the sealing
                   bulb  is opened  and allowed  to  equilibrate  at  &  reduced pressure.   In  this
                   Instance,  however.  If  it 1s seen  that  any liquid 1n the gas changer begins to
                   froth,  Indicating  volatilisation of  optional  liquid,  the  sampling  should
                   terminate  and  the pressure of  the storags container and the glass bu'J> should
                   not  be  equilibrated; a  non-representative sample of the  gas above tfte liquid
                   could result  1f  It  were 3 slxturs of liquid waste  compounds.  Pnce the bulb 1s
                   filled, the  sample  valve Is closed and Mrra1y seeled.  The bulb  1s removed and
                   shipped to the laboratory for analysis.  It is desirable to  have the glass gas
                   bulb  to be  contained   1n  a box  having  an  outer Uyrafoera  jacket  to provide
                   thermal Insulation  during handling and  for sample safety during shipping.

                        For   aas.  bag  s amp 1 1nc.  a  non-reactive  probe  1s   attached   to  the
                   high-pressure  hazardous  gas  container with  a bag  1n  the  deflated position.
                   The  tank  is  opened and  the  gas is Died  into  the gas bag,  which is allowed to
                                                           17
k

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        inflate.   Gas  bags are  usually nade  of Tedlar,  which has  been  shown to  be
        compatible with most  hazardous gas samples  collected  from the  environment  or
        froiB effluent  combustion streams.  However,  gas bag  sampling should  only  be
        used for  those  chemical  constituents for which it is validated.  Also, it  is
        Important that field blank gas  bag  samples  are  collected  at the same time  that
        the field samples are acquired.

             Fenceline monitoring  systems  are  often used  to  acquire  gaseous  samples
        which are  emitted from  open  and closed hazardous  waste  storage areas  and  to
        acquire fugitive  emissions  from industrial  plants.  Typically,  these sampling
        systeras consist  of Tenax  and/or XAO-2  sorbents through  which the  sample  is
        collected by  a  small  pump which  collect*  and concentrates the  sample  over  an
        extended  period of time.   Tne trap/sorbent  module  is  sealed  and  it  is  sent  to
        the  laboratory   for  detailed   analysis.    For  gaseous   inorganic   hazardous
        constituents,  charcoal,  and  in  some  cases,  impingers  filled with  reactive
        scrubbing solution are used to collect specific hazardous  gases.

             For  f 1 owir.q  gases  such as  that  in  incinerator combustion  stacks  or  from
        sources such  as  fossil  fuel  comhustors,  several detailed  sampling trains  have
        been specified  by EPA to  ensure collection  of representative samples  of  the
        gas and paniculate matter that may be present  in  this complex mixture.  These
        methods are  used for regulatory  purposes  to  ensure  that an  incinerator,  for
        exo.7.pVs,   does its intended  job of removing S9.995 of the  principal  organic
        hazardous constituents  (FOHCs)  in  the  hazardous  waste.   During trial  burns,
        for example,  the measurement  of  PGHCs  in the  stack gas effluent is  an integral
                                               18
v-w^-5ife^^^^
                                                                         ^«.^:^-&£<^fe-*^-^

-------
 port  of  the calculation of the destructive and removal efficiency  (ORE! values
 to   determine  whether   the  incinerator  meets   its  performance  criteria.
 Similarly,  flue -gas desulfurization  control  processes  are  sampled  by these
 procedures  to  ensure  that  regulatory  removal efficiencies  of sulfur  in  the
 fuel  are achieved.              .

      In  general,  the  sampling of a  stack gas  is the most  important  part to
 determining whether  regulatory   limits   have been   achieved.   The  sampling
 apparatus consists  of  three  major  components:

      e   An  extraction  probe  which   must  be   resistant  to  the physical  and
         chemical  reactions of  the  gas being sampled,
      e   One or  more   thermostatted  compartments  to  maintain  the  gas  at
         temperatures  consistent  with  thi collection medium,  usually    hot
         (greater  than  200"C)  for  particulate  collection,  and cool (less than
         20°C) for sorbent collection  of the more volatile constituents, and
      e   The sample  collector.

 The three major stack gas sampling trains  for  measurement of  emissions are:

      •   The Hcdified Method  5  train  (KH5).
      9   The Source  Assessment  System  (SAS), and              '
      a   The Volatile Organic Sampling Train (VOST).

 In addition, gas  bulb and gas  bag  sampling  systems have often been  used.

^t.j^^.i^^v:^                                                             .^
  ..      •              '           '•                            I              '

-------
     The  Modified  Method 5  (KHS)  sampling train  is  based on  the design  of
units which  are  used  for sampling  under EPA Method  5 (Ref. 6).   The  modified
system  (Ref.  2)  consists of  a probe,  an  optional  cyclone, a  high-efficiency
glass or  quartz fiber filter stage,  a sorbent module,  four impingers,  and some
control hardware.   A diagram of this  system Is shown  1n  Figure  1.  The  Method 5
procedure has  been modified  by Including & sorbent module  which  permits trap-
ping  of  volatile  organic  vapors  and  is  mounted  vertically  atop the  first
Impinger  of the train.  The first impinger Is empty and  is used to collect the
cof^densate which percolates through the sorbent  train module.  Details  of the
operation of  this  train  for  use 1n  samollng hazardous  waste  combustion pro-
ducts are described  1n Reference 2.
              Qjoott C?alK
                                                           Tftertaomotor
                                                                Vaoaora
                                                                Line
                                                            Vol»e
                                   Dry Qo« Alr-TigSt
                                    Mot-ar   Patae
                     Figure 1.   Modified Method 5 Train  (MM5)
                                        20


                                -Ji^.-.'jftwu, x^4^.^^^.vX^&A^3itS*^i^.-;v'.Ji
-------
     By  careful  control  of  the  temperatures   within   the   train,   organic



combustion products and POHCs are collected  in  the sorbent module.   Typically,



the  sorbent  module is  filled with XAD-2  resin,   a  porous polymer  capable  of



absorbing  a  broad  range  of  organic  chemical  species.   This  sorbent  module



provides efficient  collection of  vapor-phase  organic  materials  with  boiling



points >100°C.  An  oversized  Impinger is placed just below the sorbent module



to collect high-moisture  streams  for  subsequent organic analysis.   The second



impinger  is  a  modified  version  of  the  Greenburg-Smith   design  filled  with



scrubbing  solution.   The  selection of  the  scrubbing  solution  depends  on  the



type  of vapors  that  are suspected  of  being  contained  in  a  stack  gas.   A



caustic solution such as  sodium hydroxide  or sodium acetate is  used to collect



acidic  gases  such as  HC.1,   For collecting  volatile metals, such  as  mercury,



arsenic or selenium,  a strongly  oxidizing  solution  such  as silver catalyzed



ammonium persulfate must  be employed.  The third- impinger  is  a  Sreenburg-SmHh



impinger  with  a  tip  with  an appropriate   scrubbing  solution.   The  fourth



impinger  is  typically rilled  with  silica gel  to absorb  eny  moisture  in  the



stack  gas.   Moisture  removal  is   important  to  ensure   accurate  gas  flow



measurements  and to prevent damage to  the pumping  system.







     The  Source Assessment  Sampling  System,  first  utilized  in  1972,  is  an



alternative  integrated  stack  gas   sampling  system.   It  is   essentially  a



five-fold  scale-up of  the  HM5  train   and  collects  a larger sample, which



permits  measurement  of   lower  concentrations  of  trace-level  emissions.    In



addition, the SASS  train  also incorporates  three  cyclones and a filter in  an



oven  module   to permit   large  co1lection  capacities  for particulate  matter
               kk'^a^&^fexa r;j^'^.^

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nominally  size  classified into three  ranges:   >10v,7i, 3ym to  lO^m,  and l^m to
3vflJ.  By  means  of. a standard  142-flm  or 233-ftmi filter, a  fourth  cut less than
lyro  can  also be  obtained.  This  system is  usually used more  for industrial
sources when particularly dirty particulate emissions are generated.

     In  1982,  a  new  sampling  train,  the  Volatile Organic Sampling  Train
(VOST), was developed and  tested  and  shown  to be most effective in determining
volatile  hazardous   constituents  in  incinerator effluents.   This  system  was
developed  as  an  alternative to  the  uss of  the  integrated   gas  bag  sampling
device or  the gas bulb  sampling  system for the  collection  of volatile PCHCs.
A schematic diagram of  this train  is  shown in Figure 2.  In  this system,  the
first  trap contains Tenax  absorbent,  which  is preceded  by  a  gas  cooler/
condenser  and followed  by an  impinger for  condensate  collection.   A second
trap, containing  a   section  of Tenax and a section  of charcoal  absorbent,  is
located after the impinger.  The  purpose of the second trap is to collect very
volatile  compounds 'tertich  readily  break through  the initial   Tenax  trap.   The
method for use  cf the  VOST  also requires  reolacing both pairs  of  traps with
fresh  traps  every  20  minutes  (when  a  1-L/min  flow  rate  is employed  ovsr a
two-hour sampling period for a total  of six pairs  of traps). The serial col-
lection of several   pairs  of traps assures that the  more  volatile components
will not  pass through both  the first Tenax trap and the Tenax/charcoal trap.
The  six  pairs  of traps are  usually combined  for subsequent  desorptlon  and
analysis.

     As discussed  earlier,  it  is essential to  collect  representative samples
for  analysis.   For  the  sampling  of physical forms  of solids, liquids, gases,
                                       22

                                                               ^^

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                       Wool
                  Portlcolata Fitter
                           Ezhouot  *
                          1 M«or/ralrt
                   Coesdonoato
                  trap itaptttgor
Empty  Silica
        Gel
                                               MOTE:

                                               Botn tropo eftould be c
                                               out every 20 ralrietes over
                                               2 hoer psr'od.



                 Figure 2.  Volatile Organic Sampling Train  (VOST)
 and  combinations  in  slurries,  sludges, and  particulate-laden gases,  specific

 sampling  protocols  usually provide for acquiring  representative  samples.  After

 a sample  has  been acquired and transferred to the proper sample  container,  the

 container  must be  tightly capped  as quickly as  possible  to  prevent  loss  of

 volatile  components  and  to exclude possible oxidation from  the atmosphere.   In

 general,  samples  of  organic hazardous waste are stored  in glass  containars  and

 samples of  hazardous metals are stored in plastic  containers.  Organic  samples

 are  usually stored  at 4-6°C  to  preserve  their  chemical  composition.   Water

 samples  used  for  metal   analyses are  usually   preserved  with  nitric  acid,

 depending  on  the metals  of  question.   A discussion  of sampling and  sample

 preservation  of  hazardous  materials  in  water  and wastewater  is  provided  in

 Reference   7,   dealing  with  industrial  wastewater.   municipal   wastewaters,

 agricultural discharges,  surface water,  sludges, and  suspended  solid  samples.

                                         23
^^

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                                    SECTION 4

                                ANALYSIS METHODS

     As  r-mntione«S  briefly  1n the  Introduction,  the  RCRA  regulations require
that a  waste to  045 Identified  as  'hazardous" roust  have at  least  one of the
following four characteristics:

     (1)  Ignitability,
     (2)  Corros1v1ty,
     (3)  Reactivity, and/or
     (4)  IP Toxicity

The isethods  used to  classify a waste  for the:;e four characteristics and the
criteria  employed  are summarized  in Table  5.   Detailed procedures  for  these
laeisur-ments are given  1n Test Methods  for  Evaluating Solid Waste -  Physical/
Cfieraica'i  Methods,  SW-84&  (Ref.  1).   These procedures  are used  to  determine
whether the wastes  exhibit  the characteristics  of a hazardous waste as defined
by Sactlon 3001 of RCRA.

     Tha  objective  of the  Ignltabilitv  Characteristic is  to identify wastes
•that ara either present  fire  hazards  under  routine  storage,  disposal and
transportation,  or  are capable  of  severely exacerbating a  fire once  started.
A solid waste  is considered to exhibit the characteristic of  1gn1tab1lity 1f a
representative sample of the waste has any of the following  properties:
                                       24
«ic£j&^iA^>^-A&v.':->:-^v:--.j^

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I'-
                                    CHARACTERISTIC
ICNITAB1LITY
                     rv>
                     ui
REACTIVITY
                                                                 TABLE 5.   HASTE EVALUATION  PHOCEDURES
                                                     METHOD/CRITERIA
                    I.  Flash Point <60* -
                                                                                  •  Pansfcy Mortens  Closed Cup (RCRA  10JO) ,  or
                                                                                  •  SataH ash Closed Cup (RCRA 1020)
                                      CORROSIVITY         1.   pit *2 or J12.6 - RCRA 040,  or
                                                          2.   Corrodus SAE 1020 Steal  >6.35  emfyr  -  RCRA 1110
                     Professional  Judgement:  °
                                                                                                                          forms   potentially
Undergoes violent chemical ciienges,
Reacts  violently   with   H^O   or
explosive) mix'-ures with I^O,
Generates toxic  furtias  with  "IjO,  or  in  the cose of
cyanida or sulfio'e nsslos nhsn exposed to oildly acidic
or basic conditions,
Explodes at normal temperatures  and pressures, or alien
subjected to a 3tror:-tf  initiating  force ,:  at eleval.nd
temporflturo, or
Is a DOT Class A or Ctoss 0 Fnplosivo.
                                      EP  fOXICITY         Waste extract cocposition  exceeds  ony   of  14  specific  chemical  concentration  levels
                                                         (8  metals,  4  pesticides  and   2  herbicides);   Extraction  Procedure  (EP) defined  in
                                                         RCRA 1310;  Metal   Methods   7060,   7080,   7130,   7190,   7420,   7470.  77<0,  and  7760;
                                                         Pesticides  80GO;  and  Herbicides 8150.

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                       o  It 1s  a liquid other than an aqueous solution, containing less than 24
                          percent alcohol  by volume and  has  a  flash  point of  less than 60°C.
                       o  It 1s  not a  liquid  but is  capable,  under  standard  temperature and
                          pressure,  of  causing fire through friction, adsorption of moisture, or
                          spontaneous chemical  changes,  and, when  Ignited, burns vigorously.
                       e  It 1s  an 1gn1table compressed  gas; or
                       e  It Is  an oxidizer.

                  The objective  of  the Corrosivity  Characteristic  1s  to  identify wastes  which
                  raight pose  a   hazard  to  human  health  or xo the environment because of its
                  ability  to:

                       o  Itobilize toxic metals 1f  discharged  into a landfill,
                       o  Corrode handling,  storage,  transportation,  and management equipment, or
                       o  Destroy human  or animal tissue 1n  the event of inadvertent contact.

                  Solid waste is  considered to  exhibit the  characteristic  of  corrosivity if  a
                  representative  sample has  either  of  the  following  properties:    It   1s
                  aqueous  and has  a pH *1  or >12.5; or  1s a liquid and corrodes steel at the
                  rate of  >6.3S  ram/year  at a test temperature  of 55"C.

                       Tne  Reactivity  Characteristic of  a hazardous  waste defines  a  reactive
                  waste as one having any  of the following properties:

                       o  Readily undergoes  violent chemical change,
                       e  Reacts violently or forms potentially explosive mixtures  with water,
                                                         26
L,
                   ^


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       e  Generates  toxic  fumes  when  mixed  with  water,  or  in  the  cas?  "f
          cyanide-  or  sulfide-bearing  wastes  when  exposed  to  mild  acidic  or
          basic conditions.                                    :..
       e  Explodes when  subjected to a strong initiating force,
       9  Explodes at normal temperatures and pressures, or
       &  Fits  within  the  Department  of  Transportation's  Class  A  or  Class  8
          Explosive classification.

  Reactivity  1s  determined by  applying  the best  professional  judgements to the
  available  data.   There  are  no  explicit"  experimental   test   procedures  for
  determining this characteristic.

       The  Extraction  Procedure Toxlcity Characteristic is  determined  by a test
  designed  to simulate  the  leaching  a waste will  undergo If disposed  of  in an
  improperly  designed   sanitary  landfill.    Tnis  laboratory  test  consists  of
  extracting a  representative  sample  of  waste with distilled water maintained at
  a  pH  of  5  using  acetic  acid.  The  extract  obtained  from  the  EP  (the "EP
  Extract")  is  then  analy:r.d  to  determine  if  any  of  the  thresholds established
  for  the  eight  elements  (arsenic,  .barium,  cadmium, chromium,  lead, mercury.
  selenium,  silver),  four pesticides  (endrln,  Undane, roethoxychlor, toxaphene),
  and  two herbicides  (2,4,5-trich1orophenoxypropionlc acid, 2,4-
-------
TABLE 6.  THRESHOLD LEVELS OF CONTAMINANTS  IN  THE
        EXTRACTION PROCEDURE  TOXIC1TY T'-ST
Contaminant
Metals
Arsenic
BaMuaj
Cadmium
Chromium
Lead
Wercury
Selenium
Silver
Pesticides
EndMn
Lindane
Hethoxytiilor
Toxaphene
Kert>1c1dos
2,4-01ehlorophenoxyacet1c add
2.4,5-Trlchlonjphenoxypropionic add
Threshold Level (mg/L)

" S.O
100.0
1.0
5.0
5.0
0.2
1.0
5.0

0.0?
0.4
10.0
. 0.5

10.0
1.0
RCRA Method

7060
7080
7130
7190
7420
7470
7740
7760

8080
8080
8080
8080

8150
8150
                        28


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     In  the  extraction  procedure,  a  waste  containing  unbound  liquid  is
filtered and  if  the solid waste is less than  half  a  percent  of  the waste, the
solid  phase  is   discarded   and  the   filtrate analyzed  for  trace  elements.
pesticides  and  herbicides.    If  the  waste  contains  more than  0.5  percent
solids,  the  solid  phase  is  extracted  and the liquid  phase  stored  for  later
use.   Prior  to  extraction,  the  solid  material  must  pass through  an  O.S-RCT
standard sieve.   If the waste  consists  of  a single piece, it must be subjected
to the  structural  integrity  procedure (SIP),  which is  used to demonstrate the
ability  of the waste  to remain  intact  after  disposal.   If the  waste does not
meet one of these  conditions,  it must be ground to pass a 9.5-ron sieve.   After
extraction, the  liquidrsolid ra\'.^  is  adjusted to a 20:1  v/v  and the resulting
liquid  extract   is  separated by filtration.   The  solid  is discarded and the
liquid  extract  is  combined  with   any   filtrate  obtained  during  the  initial
separation.

     Currently,  the EPA  Office  of  Solid  Waste  is  examining  an  alternative
procedure  called the  Toxic;ty Characteristic  (.caching  Procedure (TCI?),  which
uses a  zero headspace  extractor  and generates  analysis  samples  for volatile
and  serai-volatile  organic constituents, pesticides,  and  metal  species.   This
new  procedure  is  undergoing interlaboratory  validation  prior  to  publication
for public comant.
                                       29
                        	,    .   .      ......
                    siga:a^
                     \
                     \                    •
                      \            .             '

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SURVEY ANALYSES

     The  hazardous  waste  characteristics  have  been  stipulated  as  regulatory
requirements.  Often, 1t  1s  desirable  to obtain survey Information regarding a
hazardous waste  1n order  to guide  the  detailed characterization  of  specific
chemical  species  In  the  waste.   Th.2  survey  Information  often consists  of
proximate analysis  of the waste,  as  well  as  survey  analysts of  organic  and
Inorganic species.

     Proxiraate analysis  Includes determination of  physical  properties  such as
moisture, solid,  and ash  content,  as well  as determination  of  such  chemical
properties  as the total  organic  carbon,  total  organic  halogen,  eleraantal
coar; . ivion. viscosity, and  heating value  of  the waste.   TMj latter paranseter
\r,  particularly  important when  the waste  1s to  be considered for disposal by
Incineration  techniques.   These mathods  are  listed  in  Table  7.   Proximate
analysis  provides  the data  relating  to the  physical  form  of  the waste  and
provides  an approximate  mass  balance of  Its  composition.   This  Information
meets the waste  analysis  requirement of 40 CFR  264,  Subpart 0 regulation,  and
1s  also  responsive to the general  weste  analysis  re
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                     TABLE ?.  PROXIMATE ANALYSIS Or WASTES
        Characteristic                          Method
     Moisture Content                 Loss  to constant  weight on  oven drying
                                      at 103'C for one hour.

     Solids Content                   Calculated ai  residual  weight after oven
                                      drying.

     Ash Content                      Solid  residue  after  ignition  of sajfiple
                                      at 60Q°C for 30 minutes.

     Elemental Cotnposition            Determined   by  standard   microchefljicsi
                                      Pregl train methods

     Total Organic Carbon             TOC  Analyzer  measures   C02  if-A  CH^  on
                                      combustion of sample.

     Total Organic Halide             TOX   Analyzer  measures  acic!   x-iides
                                      forrsed during comoustion of jjppte.

     Viscosity (of liquids)           Kinematic  (Ostwalrf)  Visccnseter  at  con-
                                      stant temperature.

     Heating Value                    Ad1atat1t bomb c
     Survey chemical  analyses are  designed  to provide  an  overall  description

of the  sample  i:: terras  of  (1)  the major  types of organic  comaounds,  and (2)

the major  inorganic  elements (rcetals)  that  are present.   The  survey analysis

package includes determination of:



     &  Total  organic  content by chromatographic  (TCO)  and gravimetric (GHAV)

        procedures.

     e  Organic compound class  types  present Cy infrared (18).  and  orobe mass

        spectrcroetric procedures.


                       .                31


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     9  Major  organic  componants   by   gas   chrcmatography/niass  spectrometric
        (GC/KS) or  high  performance liquid chromatographic/lnfrared (HPLC/IR)
        or   high   performance   liquid   chromatographic   ,-nass   spectrometric
        (HPLC/MS)  procedures,  and
     s  Metals  by  Inductively  coupled  argon  plasma  emission  spectroscoplc
        (ICAPJ and atomic absorption spectroscoplc  (AAS) procedures.

     The type  and data  generated  by survey  analysis  provides  a  qualitative
description  of the  overall   chemistry  of  the  sample.   TMs  information  1s
Important 1n deciding which of the hazardous constituents it, the ITD/RCRA list
are present 1n the waste, and may  lead  to  the prediction ar,fl/-<" identification
of alternative, previously unsuspected constituents in the wr.3t».

     In  recent years, the  use  of  survey  analysis procedures  has diminished
significantly  because  of  major   enhancements  1n  the   capillary   column  gas
chronatographic/mass spectrometric/data  system (CCGC/HS/DS) techniques and the
use of  specific  stable labeled  internal standards.   The  use  of improved data
system. „ target  compound  search   computer  software  has  also  significantly
Improved and   its  cost has diminished  so  that often  analysts  prefer  to  go
directly  to  a quantitative/seroi-quantitatlve procedure  without  employing  a
survey  method.   In  addition,  tha  use  and  application  of  HPLC,  improved
detection  systems  and ICAP have   also  Improved  markedly so  that  it  is  more
cost-effectlva  to  go  directly  to  the direct  compositional  analysis.   The
reader is referred to  Reference 2  for additional details regarding the use and
application of the survey'methods.
                                       32
^-^^a^^ISM^^M^ai^g^^^g^^sS^B^il^^sgfe^;

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SAMPLE PREPARATION PROCEDURES







     Samples collected  in the  field  usually roust  be treated  by  a  series  of



special  techniques  to  permit  their-  conversion   into   a   matrix   which  is



compatible  with  the  final  analysis  methods  needed  for measurement  of  the



specific hazardous  constituent.   The  techniques vary  significantly  and  depend



on whether  the hazardous  species under  question is  organic or  inorganic  in



nature, and  the  nature of the waste  itself,  whether a gas,  liquid,  or  solid.



The  sample   preparation  scheme  for  analysis  of  the organic  components  may



require  extraction  of  the  sample,  concentration of  an  extract,  and/or  the



cleanup of  a sample extract  to remove potential  interferences.  Surrogate and



standard addition methods  are  often used  to  facilitate quantitation,  determine



the degree of recovery of  the  species  in  question from the matrix, and  provide



information  regarding  the  precision  and  accuracy   of  the  resulting  data.



Digestion of a  sample  is  necessary  prior to the analysis of  metal  inorganic



constituents.  For  aqueous wastes, ii  is not  necessary  to  digest  the  sample



for metal or anion analyses.







     The  sample  preparation  method  often  depends  on  the   final  oesirad



analytical  method  of  choice.   In general,  because  of  the  high  sensitivity/



selectivity  of  fused  silica  capillary  column  GC/MS,  this procedure  is



generally   the   analytical  procedure   of  choice.    Because   of   its   wide



applicability and  generally  good  quantification capability,  this method  has



been  selected  by   EPA's  Office  or  Emergency  and  Remedial  Response  as  the



primary  procedure  for characterization  of o-ganic  constituents  in  hazardous



wastes  (Ref. 8).    In  their  procedures,  the sample  preparation  technique  is



                                       33
£&it^£^

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relatively simple  and  straightforward.   However,  if other procedures, such as
packed  column  gas  chroroatographic  methodology with  specific  detectors other
than  mass spectrometry  are  employed,  often  other  clean-up  techniques  are
required to remove  potential  interfering compounds  which  could  cause  confusion
in  the  characterization  of  the  specific  target  chemical   compound.   The
generally used sample preparation procedures are delineated  in  Table  8 and are
discussed below.

ORGANIC CONSTITUENTS

     Liquid/liquid  extraction  is  the  primary method  used  to  extract non-
volatile  and  serai-volatile  organic compounds  from  liquid  samples.   Liqjid/
solid  extraction  is  used  to  extract  these   compounds  from  solid  samples.
Hethylene  chloride  is   the   preferred   low-boiling  solvent  used  to extract
aqueous  matsrials  using either sap&ratory funnels (RCRA 3510) or continuous
liquid/liquid  extractors (RCRA  3520).   The continuous  liquid/liquid  extractor
is advantageous  compared to  the separatory funnel  method  because it  minimizes
the formation  of  emulsions  and can be performed with minimum  labor.

     The classes of organic  compounds  in aqueous-based  waste are separated by
regulating the  pH  of  the  aqueous  phase  prior to extraction  with  nethylene
chloride.  Sample  preparation  for  the pesticide/PCS constituents  In aqueous
wastes are accomplished by extraction with methylene cnloride of a  sample that
has  been  treated to  be neutral  (acidity  between  pH  5  and  9).   Separately,
sample  preparation  for  extractable  base/neutral  and  acid   fractions  are
                                       34
      M^yJateiil^^a^^

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                                      Constituents
                                  TABLE  8.   SAHPLE PREPARATION PROCEDURES

                                                                 Method
fi'l
K. .

li
                   CO
                   cn
                              Inorganic:

                                 Acid Digestion
                                 RCRA 3010; IIN03 digestion of uaiapKa; dissolvo digoatato  in 1:1 MCI.

                                 RCRA 3020; IIN03 dif)ostioii of ttampla; dissolve di floats te  in 0.63 v/v H?1Q3.

                                 RCRA 3030; Digest ion of samples containing oils,  greases, or BDMOS using
                                            and
   Organic Solvent Dissolution


   Alkaline Digestion

Organic:

   Liquid-Liquid Extraction




   Soxhlet Extraction



   Sonication Extraction

   Purge and Trap



   Head Space
RCRA 30.C0; IINOa/lioOj digssticn of sludges; digastate is aolubitized cith either IICI or
           HN03.

RCHA 3040; Use xyleno or  mothyl  isobutyl  ketone  to  dissolve  oils,  grease or «ax
           samples; organomctol I ic standards nro used.

RCRA 3060; Digestion of oarnpla cit>. No2C03 and NaOII to dotorraina Cr<5.
                                                               RCRA 3510; Adjust pli, extract «ith oothylere  clilorido using acparatory fuiinol; obtain
                                                                          three froctiona A/0/Nt dry nith Na/jSO^ and concontrato.
                                                               RCRA 3520; Alternative to RCRA 3510, but uses a continuous extractor.

                                                               RCRA 3540; Soxhlet extraction of  soils/sludges;  extract  is  dried and concentrated;
                                                                          methyfana  cliloriu'n  cthor,  acolono/hexana,  and  ber.!one/tnotl>anol  common
                                                                          extraction solvents.

                                                               RCRA 3550; AJto.i^tivn to RCRA 3540. but uses sonication to so'uhiliza sample.

                                                               RCRA 5030; Volatile organic spocies arc uuparatod  from  samp I « by purging with He and
                                                                          sorbed on Tona* sorbont; sorbont  is  then heatod, backflushcd eith Ito onto
                                                                          GC column,

                                                               RCRA 5020; Ullacjo votutae  of  vaste  container  is  sampled  using  a  gas syringe acid
                                                                          injected into CC.
I!

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accomplished  by  adjusting  a measured  volume  of  the  sample,  first  to  a  pH
greater  than   11  and  then  extracting  with  raethylene  chloride,   and   then
adjusting  the  acidity of  t.he aqueous phase to  a pH  less  than  2 and  extracting
it  with  a  separate  second  portion  of  methylene  chloride.   The  methylene
chloride  extracts  are generally  concentrated  and  dried   by  treatment  with
anhydrous  sodium sulfate and  concentrated using a  Kuderna-Danish  methodology
to a  final volume of  1.0 ml (Ref. 8),
     Surrogate   standard   spiking  solutions  and   base/neutral   acid   matrix
 standard  spiking  solutions  are  employed  to  permit  calculation of  (1)  the
 aqueous  soil surrogate  percent recoveries,  (2)  the matrix  spike and  matrix
 spike  duplicate  percent  recovery  results,  and  (3)   the  relative  percent
 difference  between  duplicate  analyses.   A method  blank  is run  concurrently
     r                         '
 using  an  equivaTent volume of  deionized  distiller, lasor?.tory water  for  water
 samples,'  or a ourified solid matrix for  soil/sed-ment  samples  carried  through
 the  entire analytical scheme  of  extraction, concentration and  analysis.   The
 metnod olank  volume or weight  must be  approximately equal  to sample  volumes or
 sample  weights   being  processed.   Surrogate   standard   determinations   are
 performed on  all samples and blanks.

     All  saraples and  blanks  are  fortified with surrogate  spiking  compounds
 before purging  or  extraction  in  order  to monitor  preparation and analysis  of
•samples.   In order to  evaluate  the matrix effects of the  sample upon  the
 analytical  methodology,  the  USEPA has  developed  standard mixes  to be used  for
 matrix spikes and matrix  spike duplicate  analyses.-  The surrogate spike  method
                                       36
    ^^^M^^^^£^^^^^s^^:^£i.^^^^
                        \

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blank  and  matrix  spike  duplication  analyses  are i  -d  as  Quality  assurance
procedures  to  ensure  that  the  data  generated are  complete,  representative,
comparable, valid, of kncun precision and accuracy, and legally defensible.

     The CERCLA  regulatory  procedure-  for  preparing  soil  sables  consists of
ultrasonic   extraction  of  dried  soils/solids  with  methyl?;ne  chloride  after
surrogate  standards  are  added  to  all  samples,  spikes  and  blanks.   A matrix
standard spiking  solution is added to  two 1-gtn  portions  of  the  sample chosen
for  spiking.   After sorsication for two minutes at  100-vatts power with pulse
set at 50 percent., the  methylene  chloride extract is separated from the soil by
filtering  through  glass wool and then  concentrated to a  final volume  of  1 ml
by & nitrogen blow-down technique.

     Pargeable  (volatile)   organic  compounds   in  these • samples  are  first
screened  on  a  gas  chroraatographic/flame  ioniration  detector  (GC/FIQ)  to
determine  the  approximate  concentration   of   organic   constituents  in  the
samples.   The  actual  sample  preparation is based  on a  purge and  trap method
(RCRA  5030).   For  the sediment/soil samples, the  purge  device  is heated.   For
water  samples,  an inert  gas  is  bubbled through  a 5-rL  sample contained  in a
specifically designed  purging chamber  a*,  ambient  temperature.   The  purgeable
constituents are  efficiently transferred  from  an  aqueous phase  to  the vapor
phase.  The  vapor is  swept through  a  sorbent  column  where the  purgeables are
trapped.   After  purging  is  completed,  the   sorbent column  is  heated  and
backflushed  with   an  Inert  gas  to   desorb   the   purge&bles   onto   a   gas
chromatograohic  column.  The  gas chromatograph  is  temperature   programmed  to
                                       37
 .-..."-,.      .     ,<,-••    •   •••-'  ••'- -            -• '  •' •--

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             separate  the purgeables-which are then detected with a mass spectrometer.   For
             sediment/soil  samples, an  Inert gas  1s bubbled  through  a mixture  of a  5-s
             sarcple and  reagent water  contained  in an especially  designed  purging  chamber
             maintained at  elevated temperatures.

                  For  sorae  samples, the level of  Interfering compounds  is sufficiently  high
             to preclude successful  analysis of  the  analytes  of Interest.   For  these
             samples,  one  or  more  clean-up  steps  should  be  considered to  facilitate  the
             final  analysis step.   Clean-up,  methods  such  as size.exclusion  chromatography,
             liquid column chromatography, using columns  filled with  silica  gel,  Forisil,
             activated  alumina,  charcoal, etc.; solvent partitioning and filtration  may  be
             used  alone  or  in coraijlnacion to cleanup  the samples for  analysis.  A  ceranon
             solvent   partitioning  technique*  used  for   the  cleanup   of   polychlorinated
             biphenyl   compounds   consists  of  treating   the   sample   with   a  mixture   of
             concentrated sulfurlc add  and hexane.   In this case,  the  PCBs  are partitioned
             into  the  hexane  layer  and  aqueous constituents and  many  organic compounds  are
             retained  in the  sulfuric  acid  layer  by reacting with  the sulfuric acid  and
             farming a  sulfuric acid soluble  product.

             IMORSAWIC  CONSTITUENTS                         '     "

                  Preparation  procedures   for all   wastes  containing  metals  include   a
             digestion  step unless  it  1s  an  aqueous waste  and can be  used  directly.   The
             digestion   procedures,  RCRA  Methods  3010,  3020.  3030,   and  3050,  are acid
             digestions,  with  varying degrees of  acid strengths and oxidizing capabilities.
                                                   38
i^lfe^^^

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  Alternatively,  oils,  grease and  waxes  can be  solubilized,  often using  xylene
  or  methyl  Isobutyl  ketone as solvents.   In this case, organometallic  standards
  are used  for  the metallic  species.   In  the  special case  of  determining  the
  amount  of  chromium 1n the  +6  valence  state,  alkaline digestions are  employed,
  using basic carbonate media.

  ORGANIC  ANALYSIS  METHODS

       The  EPA  Superfund  (CERCLA)  regulatory   procedures  consist  of  using a
  comprehensive   capillary  column  gas  chromatographlc/mdss   spectrometric/data
  system  technique  for characterizing a  wide range  of analytes  (Ref.  8).  This
  has been proven to be the most cost-effective way  to characterize a wide range
  of  analyte chemical  classes.  As discussed  in  the sample preparation  section,
  the wastes are Isolated  into  four separate fractions by extraction  and  purge
  and trap  techniques.   These  fractions,  the  pesticide  fraction,   the acid
  fraction,  the  base/neutral fraction,  and the volatile  organic constituents
  (VOCs)   fraction  a-e  analyzed  by  capillary  column  gas  chromatographic/mass
  spectrometric/data system (CCSC/MS/OS) techniques.

       The CC6C/KS/DS. method  is extremely powerr'ul   because  it can provide both
  qualitative and jemi-qualitative results.  The  mass  spectrometer used must be
  capable  of scanning  from 35 to  500 amu  e>,;*v  one  second or  less, utilizing 70
  volts  nominal  electron  energy   1n  the   electron   impact  ionization  mode  and
  producing  a  nwss  spectrum  which  meets  all the  requirement's and criteria when
  50  ng  of   decafluorotripheny Iphospfiine   (0CTPP>   is   injected  through  the  GC
  Inlet.   A  computer data  system  must be  interfaced with the mass spectrometer
                                         39
j^^                                                '-

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                that .allows continuous  acquisition and  storage on  machine-readable  media of
                all  mass  spectra  obtained  throughout  the  duration  of  the chrosnatographic
                program.   T.ie  computer must have software that allows searching any GC/MS  data
                file  for Ions  of specific mass and plotting such ion  abundances versus  time or
                scan  number.   This type of plot 1s defined as  an extracted 1on current  profile
                (EICP).   Software roust  be available that alloys  integrating the abundance in
                any  EICP between specified time tr scsn r.uwUr- limits..

                     A key factor 1n the  use of  computerized  r::'.ss  spectra search systems 1s
                the  data  base.   Tentative identifications  are obtained  from the GC  relative
                retention time  Information and the  examination of  specific mass spectra  for
                the  individual gas chroraatographic peak  of either  a  pure compound or  certainly
                a limited num&er  of  confounds,  and  comparison   with  the  data  base  usually
                provides  uneculvocal  characterization  of  the  ccrnpounds.   The  computerized
                reverse-search systems have been enhanced so  that  a  series of target  compounds
                can  be  Identified with search  routines  requiring  less  than throe  seconds per
                target compound (e.g., a-search of TOO compounds in less than five minutes).

                     Algorlthras  for  goodness-of-flt  parameters and  the  values  associated  with
                specific  levels  of  confidence  in  the  identification vary,  depending  upon the
                particuUr software  employed.  For  this reason,   it 1s essential to  also use
                the  professional judgement   of  the mass  spectroscopist  to  verify  that  all
                compound  identifications are  accurate.
                                                        40
I.     V
fcii^&I&aE^

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      Since 1980, the use of  stable  labeled  surrogates  as  internal  standards in
 combination  with  the  CCGC/MS/OS  characterization of  pollutants  has  been  a
 further  significant   enhancement   of  the  analysis  of   samples   containing
 hazardous  compounds.    In   this  method,  the  stable  labeled  analog  behaves
 chromatographlcally   Identical   to   the  target  compound;   however,  its   mass
 spectrum  is  clearly  distinguishable  from  the   non-labeled  compound  in  the
 sample.   In EPA Methods  1624 and 1625 (Ref. 9),  a total of 32 and  65  s~?cific
 stable labeled  Isotopes, respectively, are used in an  isotope dilution  mode as
 internal   quantitation   standards.   This  approach  has  resulted  in enhanced
 precision and  accuracy  of   analysis;  it has  also  been  determined  thet  the
 calculated  percent recoveries using  Isotope dilution are uniformly  unaffected
 by  the sample  matrix.   The  availability  of stable  labeled analyte standards
 has   increased   significantly since   Its  Initial  examination   for pollutant
 analysis  purposes.   The commercially available useful stable labeled compound:
 has  grown from  36 to  over  107,  and 1t  appears that  additional  compounds will
 be  available  to support  the  analysis  of many  of  the  pollutants  listed  in  the
 ITO/RCRA  list (see Appendix).

      Detailed CCSC/MS/OS  procedures  for the  analysis  of chlorinated dibenzo-p-
 dioxlns  and  dibenzofurans  are  given  in  RCRA Hethod  8280  (Ref.   10).   This
 method  utilizes  an  analytical   extraction  clean-up  procedure,  a  CCGC/MS/DS
 method   and    7C1   stable   labeled    internal   standards.    If   interfering
 substances  are  still  presen-c after the initial  clean-up  steps, the analyses
 are separated from the interfersnces using an HPtC clean-up procedure.
S^^^^

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     Hany of the  high-molecular weight,  non-CCGC  separable compounds listed 1n


the Appendix can  be  analyzed  by  high-performance  liquid chromatography (HPLC).


This method  uses  specific  hardware  consisting of  reservoirs for  the  elution


solvent(s) which  may have a system for  blending  two  solvents using a gradient


mixing  device,   pumps,   injection  port,   columns,   detection,   and  rsad-out


devices,  and  thermostats for  the  colutsn and  detector.   These  components  are


consBercially  available  as  Individual  modules  or  for  incorporation  into  a
                     «
complete  HPLC  system.   The  most common  HPLC detectors  utilize  ultra-violet


absorption  or  fluorescence  emission   at   a   single  wavelength.   Polynuclear


aromatic  hydrocarbons  are often  analyzed  by  HPLC  methods whon those  are  the


primary constituents in the waste (RCRA Method 8310).




     Another  analytical   method  that  is  receiving  considerable   Interest  in


analyzing complex mixtures  is one of  liquid  chrofratography/oass spectrorcetry.

In this case,  a  separation  'Of non-volatile materials  occurs  by  liquid chroiw-


tography  and  then a thermosprgy  injection  technique  is  used  for  introduction


of the  liquid  compound Into the mass  spectrometer.   This advanced methodology


is currently under  considerable  research at the  present  time.   It Is believed


that sorse analytical procedures for specific  compounds  will  be recommended  for


use 1n the near future.




KONITORIHG




     For  many  hazardous  wastes  generated  routinely  in industrial  operations,


or where  the waste  is  relatively well  known,  monitoring techniques can be most


useful!   In  this case,  the  high-resolution,  comprehensive  capability of  the


                                       42

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CCGC/MS/DS  1s  not  required  and  less  sophisticated  and  less  costly  methods,
such as  packed  column gas chromatography with  specific  detector capabilities.
can  be  'employed  successfully.   These  methods  were  initially  tested  and
validated  for  use  in characterizing  organic  wastes in wastewaters,  surt'aca
waters and  industrial  discharges to satisfy  the Clean Water  Act requirements
and  the  National Pollution  Discharge  Elimination  System  (HPDES).   Procedures
coftsnonly  used  for  monitoring  organic   constituents after   use  of  specific
clean-up methodology are listed in Table 9.

INORGANIC CONSTITUENTS

     Inorganic  constituents   of  wastes  are  categorized  as   metal  or  metal-
containing,  anion-containing,   or gases.   Met.jl-containIng  species in  wastes
are  usually analyzed  by  atomic  absorption spectroscopy  (AAS)  or  Inductively
coupled  plasma   emissions   spectroscopy (ICAP)   techniques.    Two modes  of
analysis are used for  these species;  direct  analysis from solution,  or coal
vapor/hydride evolution.   The  choice  of analysis  technique  depends  upon the
specific metal of interest and  required detection sensitivities.

     For all  the metals,  except  arsenic,, selenium, and mercury, the  solution
resulting  from  the digestion  preparation procedure may be aspirated  directly
Into the flama  AAS  or into the plasma for  ICAP,  or injected  directly  into the
furnace  for Nameless AA  analysis  at a wevelength  which  is  specific  to the
element  under  Investigation.   The  spectrometer is adjusted  so that  only the
specific  wavelength(s)  of   interest  are   detected   at   the   photomultiplier
detector.  The amount of absorption or emission which occurs  during the AAS or
ICAP experiment  Is directly related to the concentration of the metal present.
                                      43   .

-------
j
V
                                                 TABLE 9.   RmJTINE/KOH/TORIKn ORGANIC ANALHICAL  KETMODS
            Organic Spocies


llalogenalod Volctlle Ccejx/undc,

Volatile Organic Compound*

Volatile Aroootic Compounds

Acroloin, Acrylonitrilo, Acetonitrilo

Phenols


f'hthatato Ester*

Organochlorido Pesticides ft PCOa

Ni'.ro arooatic compounds end
Cyclic kgtones

Polynuclear Arcaotic Compounds


Chlorinated Hydrocarbons

Qrganophosplwruo poalicidos

CMori.;atod Herbicides
                                                                                                       Method


                                                                  RCRA SOlO-Puryo end trap Injection irito pecked cnluon CC/CCD

                                                                  RCIIA OOlS-Puroo and If no 'r. joe I ion into packed column progrr.CTt.od CC/I ID

                                                                  HCBA 80?0-Pjf6O end trap Injection into packed coluan progrnoraod CC/FJO

                                                                  RCRA 8030-Purr
-------
     For  selenium  and arsenic,  the solution  resulting  from the  digestion of
the  sarr/ple 1s  treated w4th  stannous  chloride to  forra  Intermediate  reduced
species,   As02   and   SeO,.    The   solution   1s   then   treated  with   zinc
rectal, converting the  reduced  species  to  the volatile hydride.   The hydride 1s
then detected by the  A.AS  method.   For rsercury, the solution resulting from the
digestion  of  the saaple  1s treated with  stJp.nous sulfate, which  reduces the
Ionic  csrcury  in   the sample  to  the atomic  species.   The  volatile  atomic
raercury 1s swept from the sample in a closed system to an absorption cell to a
scrubber  trap.   The level  of  (cercury  1n  the vapor is  obtained  from  the Inte-
grated AAS signal foraad during ns evolution fron the Sereple.
     External calibration curves £ -e  prepared  by plotting the absarbance (AAS)
or transmittance  (IC/'-f-J  versus concentration  for a series  of  standards which
span the  linear working  range of the analytical  Instrument.  On comparing the
measured absorptions  (or  transmittance)  of the  sample  analyzed  under the sam?
conditions as trie  standarti,  the  concentration  of material in the sample can be
interpolated from  a calibration  curve.   Table  10 lists  the KC2A procedure used
to characterize the hazardous metal content of. wastes.
     SOJES of the  inorganic  species listed 1n  the  ITO/RCRA list (sec Appendix)
are  hazardous  because  of  the  anionic  portion  of  the  confound.   These  com-
pounds. which contain either cyanide,  phosphide,  or sulfide,  are analyzed  by a
single method for  that  anion.   The general  procedure  for  the determination of
anions  in  solution  employs  1on  chronatography  as  the  preferred  analytical
technique.  It should be  noted  that  some of  the  sample preparation methods can
                                       45

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TABLE 10.  RCRA METHODS FOB RETAL ANALYSIS OF WASTES
RCRA Method Number
Ketal
Antimony
Arsenic
Bariura
Beryllium
Cadmium
Chromium
Copper
Lead
Mercury
fHcfcel
Osnri urn
Selenium
Silver
Thallium
Vanadium
Z1nc
*€aseous Hydrlda
**Cold Vapor
AAS
7040
7061*
7080
7090
7130
7190
7210
7420
—
7520
7550
7741»
7760
7840
7910
7350
Kethod

AAS-GF
7041
7060
7081
7091
7131
7191
7211
7421
—
7521
7521
7740
7761
7841
7911
7951


ICAP Other
6010
6010
6010
6010
6010
6010
6010
6010
— 7440**
6010
6010
~
6010
6010
6010
6010


                          46

                                                                         fcaaesa;

-------
                convert  these  compounds to  volatile  species, which  could  be removed from the
                waste    inadvertently.   Care  must be  exercised  during  the  sample treatment
                effort   to  either   intentionally  trap  these  volatile  species  or  use  an
                alternative method   (alkaline  digestion/extraction)  to  ensure  their retention
                in the sample.

                     Scrubbing  the  effluent  from  the  acid  treatment  of  waste   containing
                cyanide  with sodium  hydroxide  solution  permits retention of the cyanide, which
                subsequently can  t
-------
                                   SECTION 5
                  QUALITY ASSURANCE AND QUALITY CONTROL PROCEDURES

     An  essential  part of  any  sampling and  analysis  program 1s the provision
for  procedures  which maintain the quality  of the data throughout the sampling
and  analysis effort.   The  level  of  quality assurance  applied to  a specific
activity  depends upon  the  project  objectives and  the  end  ^ses  of  the  data
generated.   Usually,  a flexible  program  is  generated which  also  ensures  that
all  data  are  of  sufficient  and  appropriate quality  to  meet  sampling  and
analysis  project requirements.   It is essential  that  these  data are complete.
representative,  comparable,  valid,  of  known   precision  and  accuracy,   anu
legally  defensible.   Quality assurance  (QA), therefore,  represents  the total
Integrated  program  for  assuring the reliability  of monitoring  and measurement
information.   The  assurance  of  this   reliability   1s,   in  turn,  maintained
through  the  use of  discrete quality  control  (QC) functions  wnlch involve the
routine  application  of  procedures  for  obtaining  prescribed  sampling   and.
analysis standards of performance.

     The  US  EPA has  established a requirement that  all  measurement activities
are covered  by  a Quality  Assurance Project Plan (QAPP).   This section provides
a brief  description  of the  essential  elements to this plan  which satisfy the
mandatory EPA requirements  (Ref. 11).  These  16  essential elements  are  listed
1n Table  11.  The  first three elements of  the QAPP  are  self-explanatory.   The
project description  is typically presented  in some detail, whether the plan be
primarily an analysis of  waste  provided  by EPA   contracted  sampler  organiza-
tions,  or the  activity  be  an  application  of  a control  technology such  as
                                       48
                                                               ; ;'^^I^

-------
                              TAbLE 11.  ESSENTIAL ELEMENTS OF A QA PROJECT PLAN
                          1.         Title Page
                          2.         Table of Contents
                          3.         Project Description
                          4.         Project Organization and Responsibility
                          5.         QA Objectives
                          6.         Sampling Procedures
                          7.         Sample Custody
                          8.         Calibration Procedures and Frequency
                          9.         Analytical Procedures
                         10.         Data Reduction, Validation, and Reporting
                         11.         Internal Quality Control Checks
                         12.         Performance and System Audits
                         13.         Preventive Maintenance
                         14.         Specific Routine Procedures Used to Assess Data
                                     Precision, Accuracy, and Completeness
                         15..        - Corrective Action
                         16.         Quality Assurance Reports to Management
                incineration  or landfilling.   A  brief summary  of  the  project, a  list  of  the
                waste  to be  treated,  specific  analyses  to  be  performed, and  target  analyte
                detection limits are usually provided.


                    In  the project organization  and responsibility section,  Individuals  who
                have  responsibility  for  the  following   functions  in  specifying  the  QA/QC
                program are identified:
                                                      49
L&^v^lfe^.;^

-------
          e  Project  Manager,


          o  The  Quality  Assurance  Coordinator,
                 i

          0  The  Analysis Coordinator,


          o  The  Sampling Coordinator, and


          e  The  Quality  Control and  Sata Manager.




                                                               *

     These individuals all  have specific  functions  in  conducting  the  measurement


     activities which need to  be described  in the QA Project Plan,






          The quality  assurance  objectives  of the  measurement activity  are  sum-


     marized  in  terms of  precision, accuracy, completeness, representativeness,  and


     comparability  for  each  measurement  parameter.   Quality  assurance  objectives


     for accuracy and precision will' be based on prior knowledge of the measuremint
                   '                                               «,

     system  employed  and  methods  validatio'/i • study  using  replicates,  spikes,


     .standards,  calibration,  recovery  studies,^ etc.,  and  the  requirements  of  the


     specific effort.






          For each  major measurement  parameter^},   including  all  pollutant  mea-


     surement systems, the  sampling  procedures  will  be  described.  To  be included


     are descriptions of  techniques or guidelines, use  of  selected  sampling sites,


     inclusion of  specific  sampling  procedures,  charts,  flow diagrams  or tables


     delineating  sampling program  operations,  and  a  description  of  containers,


     procedures,  reagents,  etc.,  used  for  sample  collection,  preservation, trans-


     port and storage.  Also included are special  conditions for the preparation of


     sampling equipment  and  containers,  sample  preservation  methods and  holding
                                            50
£^ai^lsa*&^                                                                             .

-------
               times,  time  consideration  for  shipping  samples,  sample  custody  or chain-of-
               custody  procedures, and  forms,  notebooks  and procedures  to  be used to record
               the  sampling  history,  sampling  conditions, the analysis to be performed.

                    Sample custody information is  required, and when used for legal purposes.
               "chain-of-custody"   procedures  must  be  described.    At  a  minimum,  detailed
               documentation of   procedures  for  field  sampling  operations  and  laboratory
               operations are required.

                    Calibration  procedures and  frequency informatijn is needed  for  both the
               sampling  and  analysis  efforts.   Incorporated  in  the  QAPP  for  each  major
               measurement   parameter,  including  all   pollutant   measurement   systems,  is
               information  on the frequency  plan for  recalibration, as well  as  calibration
               standards and their sources.

                    For  each major measurement parameter, including  all pollutant  measurement
               systems,  standard operating analytical procedures need  to  be  citetf or written
               descriptions  given. '  Hany  specific  analytes have  yet  to  be valitisted,  and
               hence,  QC data on  analysis of  surrogetes,  duplicates and spiked samples serve
               as  indicators of  the  performance of  the  sample preparation and  analytical
               methods.

                    Explicit information  is  required in  the  QAPP  regarding  data  reduction.
               validation   and    reporting   procedures.    For  each   measurement  parameter,
               including  all pollutant measurement systems, information is required regarding
                                                      51
32siteM!^^

-------
the planned data reduction  scheme  to be used to calculate the concentration or
value of  the  measured parameter and reporting units.   The  principal  criteria
that will be used to  validate  the  data integrity should be reported as well as
tBethods  used  to  Identify  and  treat  outlying data.   Data  flow  or reporting
sche
-------
     The following  types  of preventive maintenance  items  should  be considered
and addressed 1n the QAPP:

     o  A  schedule  of  Important  preventive maintenance  tasks  that must  be
        carried out to  minimize  downtime of both  the  sampling  and measurement
        systems, and
     e  A list  of any  critical  spars parts  that  should  be on  hand tn minimize
        downtime.

     A series of  specific routine procedures must be  developed  and documented
to  assess  data  precision,  accuracy,  and.  completeness.   Mean  values  and
estimate  of precision  are  provided  by  normal  statistical  means  using  the
relative  standard  deviation  as   the  precision measurement.   The  accuracy  is
assessed by mean  recovery of surrogate compound  and/or,  in the  case of  stable
labeled  compound   (e.g.,  Method  1624/1625),  by  use  of  the  stable  labeled
standard addition analyts.  -When  it is determined that  the causes of variance
need  to  be  assessed,   it  is  accomplished  vypically  using  the   sampling  and
analysis procedure  shown in Figure 3.   The analysis  of a  minimum of  seven
samples  prepared  as shown  in Figure  3  penults  estimation of  the  causes  of
variance from cither sampling, preparation and measurement (Ref.  12), e.g..
              s2    '. s2        + s2           -i- s2
               Total =  Sampling    Preparation    Measurement
                                       S3

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                                        Preparation   Analysis
                    Figure 3.   Diagram of a sampling and analysis procedure which uses
                     replicate sair.ples to  provide  information on sources of variance
                  Corrective action  procedures must  be described  for each  project,  which
             Includes  the following elements:

                  o Predetermined limits  for  data  acceptability  beyond  which  corrective
                    action  1s  required,
                  • Procedures for corrective action-,  and
                  a Identification  of  the   responsible   individual   for  initiating  the
                    corrective action  and  the  individual  responsible  for  approving  the
                    corrective action,  1f necessary.
                                                    54
sai
  ^IiH^'>...;> irt-^J^jl&MJ^^^^^

-------
Corrective actions  may  also be  initiated  as  a result of  other  QA  activities,



Including performance audits,  systems  audits,  laboratory/interfield comparison



studies,  and  QA  program  audHs  conducted   by  the  EPA  Quality  Assurance



Management Staff.







     Quality assurance reports are  initiated during  regular  meetings  among  the



Quality Assurance Officer,  the Project Manager, and key  staff  responsible  for



sampling, analysis,  QC,  and data management  to review the  QC data summaries,



documentation ar.J other  aspects  of the project  quality  assurance  performance.



The Quality Assurance Officer's  assessment of the adequacy  of  project  quality



control/quality  assurance  performance  1s then   summarized  in  a  memorandum



distributed to  upper  corporate/institutional  management,  as well  as  to  the



Project Manager and  the cognirant line management.
                                       55


-------
                                                     REFERENCES

                   1.   'Test Methods  for  Evaluating  Solid  Waste  -  Physical/Chemical  Methods."
                       SW-84&,  Sacond Edition,  U.S.  Environmental  Protection Agency, Washington,
                       D.C., 1982.

                   2.   Harris,  3.C., D.L.  Larsen,  C.E. Rechsteiner,  and  K.E.  Thrum, 'Combustion
                       of Hazardous Wastes  -  Sampling  and Analysis Methods," Hayes Publications,
                       Park Ridge. NJ,  1965.

                   3.   Proposed  Sapling  and  Analytical   Methodologies   for  Addition  to  Test
                       Retnods  for  Evaluating Solid Haste  -  Physical/Chemical  Methods.  5&-S46,
                       Setond  Edition,  U.S.  L'nvironmsntal  Protection Agency,  Washington,  Q.C.,
                       1984.

                   4.   40 CFR 261. Appendices III, VII, VIII, X, July 15. 1985.

                   5.   W.E.  TelHard,   ITD/RCEA  Compound  Analyses,  Privete  Communication,  21
                       October 1985.

                   5.   40 CFR 60. Appendix A (1980).

                   7.   Handbook  for Sampling and  Sample  Preservation  of Water  and Wastevater,
                       U.S. EPA Environmental Monitoring and Support Laboratory, Cincinnati, OH.
                                                         56
t>.,-.. ^•,-x,r.".^,.^""--/;5r-  "   '•-"..  ""••-.    -   ~   ~~~~~'"    -        -    "

-------
 8.  US  EPA  Contract  Laboratory  Program.  Exhibit 0.  Analytical Methods  for
     Organic Analysis; Hultlmadia/f-iultlconcentration.  1385.

 9.  Rethod 1624,  Volatile Organic  Corepounds by  Isotope  Dilution GC/MS.  and
     Method 1625,  Semi-Volatile Organic  Comoounos  by Ir.otope  Dilution  GC/HS,
     49 Federal  Register 43234,  October 16, 1984.

10.  40 CFR 261, Appendix X, Juiy 15, 1985.

11,  Interim  Guidelines  and  Specifications  for   Preparing  Quality  Assurance
     Project  Plans,  CAMS  005/00,  Office of  Monitoring  Systems and  Quality
     Assurance,  Decentber 29, 1980.

12.  B-H.  Colby and  a.£.  Picker,   "EstaolisMng  Destruction  Efficiency  for
     Hazardous  Waste   Incinerators,0  Submitted to  ASTO Journal  February  27,
     1984.
                                       57
                                                  £^^^                                     -.

-------
                                    APPENDIX

     This apoe.-dix  is  a comprehensive  compilation  of specific coraoounds  that
have been 1dent1,M««i as hazardous in  EPA  regulations, or  in  proposed  additions
to regulations thav nay exist  in. waste  materials  (Ref.  5).   This  list includes
all cofispounds  1n the  RCRA  Appendix VIII  list, the  proposed addition to  that
list  (N1'-hio»ft  Petition),   the CERClA  Hazardous  Substance  List,  the  Priority
Pollutant  U*«t.  -Appendix   C   Pollutants,   and  High  Priority  Paragraph  4(c)
Pollutants, together with  confounds  not  specifically identified  in  the  llscS
'ited above   but  are covered  by compound  class citations in the  Appendix  YIU
11st    The  empirical   formula  and  CAS  registry number  are   presented  for  eacn
coispW-d.  together  with-an indication  of  known  analysis methods or probable
applicable  aethods.  the promulgated  EPA  nssthod,  and applicable RCRA method.
vhen known.

     Analysis and other information is  coded 1n the table as shown below:

     CVAA      *>' Cold  vapor atomic absorption spectroscopy

     DiOXIM    « Analysis for  dibenzo-p- 6as chroiEatography with  electron capture detector

     SCHS      ° Sas chromatography/mass  ipectrotnetry

     S(;-^?0   = Gas chronatography with  nitrogen-phosphorous detector

      KPLC      »  H1qh  performance liquid  chromatography

      HPLC-UV   = HPLC  with  ultra-violet detector

      JCP      . inductively  coupled  argon plasma soectrometry

      MAS      - Determined using Master Analytical  Scheme

      K5-PK08   • Probably  determined  using mass spectrometry

      KO SCJ^   - Cannot be determined using SCMS

      TEH      - Transmission electron microscopic  analysis

      y£T       " Classical wet method

      SRC -     Denotes this  analyte  will  be identified  by  computer  search  of
                an analyte-specific  library in 6CMS data

      H -       Artalyte hydrolyzes in water
                                        58
         aa^aJ^iSk^^^^
                                                             I      :  •

-------
w^r.w - •
•i \
1
f" J
H'-L
^ "• ' '
$$
1? '
&'•
!V .
IV'
* * '
b" • i
[Jr
,''"'..'
;"r
I .', /
"i' r"
I?'''.
1'
i: •
1:
^.
v
A
*
i':



Namtt in Regulation
Acenophlhenu
Acenaphthene, 5-nitro
Acoriaphthy lene
Acetnraide N- (4-5-ni tro-22-f ury ))-
Uiiazolyl)
Acetic acid, (4- [bis(2-chloroethy 1)
ami no] plicmy 1 ) -clio 1 estory 1 estor
Acetoni Lr i lo
3- (a Ipha- Ace tony 1 benzyl ) -4-
hydroxycoumar in and salts
AcelophoMOite
AcoLyl chloride
1-Acel.y 1 -2- tli ir. urea
2-A.cety lami nof luorono
Acroleiri
Aery 1 amido
Aery loni tr i lo





Table A.I ITO/RCRA f.OMPOUIJD DATA
Emfiricol Arta lysis RCRA
forp.ulo CAS Number Typo Molhc/d GeUiod Other
C12!!io 83-32-9 GCMS 1626 0270
C12HgH°2 602-67-9 MS-PROO SRCH
C1?H8 208-SG-9 CCMS 1625 8270
C0II7N302S 631-02-8 HPLC
C30!I59CI2H02 35-16-10-9 ItTLC
C2!I3N 75-07-8 CCUS SRCH
C13!lJ604'Na 129-06-6
C0i!00 08-85--2 MS-PHOO SRCH
C2II3CIO 95-36-5 -- — II
C3H6N2OS 591-08-2 H5-PROQ SRCH
clb"j3NO '1V364-30-6 MS-PROD SRCH
C3H40 107-02-8 GCMS 1624 82-10
C3H3N 79-06-1 MAS SRCH
C3M3N 107-13-1 GCHS 1624 8240
Ed



-------
ToMo A.I   ITD/RCRA COUPGUHD DATA (Continued)
Nome in Regulation
Actinonycin 0
Af Is toxins
Aldrin '
Ally) alcohol
Aluminum phosphide
(hydroxym othy 1 ) -8a-raethoxy-5-methy 1 -
carbamata az irino[2* ,3* :3,4]pyrrolo
[1 ,2a] indole-4,7~dione, (ester)
3-Amino-9-ethyl carbazolo
4-Aminobipheny 1
5- (ami nomothy 1 )-3- isoxazolol
Amitrole
Ammonium salt (of saccharin)
Ammonium, (4-(p-(dimethy lamino)-alpho-
Empiricol
Formula
C62H86W12°16
C17nl2-l°6-7
C12H8CI6
c3»6o
AIP
Cl5»10f«4°5
Cj2H,4N
C12llnN
C4H6N20
C2H4N4
C7H5N03S»H3N
C23II2,N2.CI
CAS Wunber
50-76-0
1402-62-2
309-00-2
107-18-6
203S9-73-8
60-07-7
132-32-1
92-37-1
2763-96-4
61-82-G
6301-61-9
569-64-2
Anglyaio RCRA
Type £iothod MothotJ Otlior
HPLC
Nf;-GO(S —
CCEC 608 0080
MAS SRCH
ICP — 1610
HPLC-UV —
MS-PROB SP.CH
MS-PROB SRCH
HPLC
__
H
—
  phenyl benzylidine)-2,6- cyIcohoxadion-
  1-yIidene)-dimethyl-, chloride

Aniline                                  ^G"?^
                           62-63-3
CCMS
SRCH
                       60

-------
Teble A.I   ITO/RCRA COMPOUfO DATA  (Continued)
Name in Regulation .-.
Aniline, 2,4,5-trimethyl-
Aniline, 4,4'-mothy lenebis (2-methy 1}-
Aniline, 4 ,4 '-methy lenebis (N,N-
di methy 1)-
Aniline, 4,4'-thiodi-
Aniline, p-(pheny lazo)-
o-Anisidino
o-Anisidine hydroch 1 or i do
o-Anisidine, 5-mcthyl
o-Anisidine, 5-nitro
Anthracene
Anthraquinone, l-amino-2-roethy 1
Anthraquinone, 2-amino
Anthraquinone, 2-methy l-l-ni tro
Antimony
Antimony (I I I) chloride
Empirical
Formula
C9H13N
Cl5H18N2
C17M14M2
C12H12N2S
C6llnN2
CgllgNO
C9II10NCIO
C10HHNO
C10H0N203
C14fi10
C15"lO
C14II9N02
C15H9N04
Sb
SbCI,
Analysla RCRA
CAS Number Type Method Method Other
1377-17-7 MS-PROD
838-00-0 MS-PROD
101-61-1 MS-PROD
139-65-1 IIPLC
60-09-3 HPLC
90-04-0 NS-PROD
134-29-2
120-71-8
99-59-2 MS-PHOB
120-12-7 GCMS
120-12-7 GCMS
117-79-3 MS-PROD
129-15-7
7440-36-0 FURN-AA
10025-91-9 FURN-AA
SRCH
SRCII
SRCH
--
--
SRCH
H
II
SRCH
1625 8?70
1625 8270
SRCII
--
7041
7041
                       61

-------
Tnbla A.I   ITD/RCRA COMPOUND DATA (Continued)
Namo in Regulation
Antimony (V) chloride
Araroi bo
Arsenic
Arsenic acid
Arsenic pentoxide
Arsenic trioxido
Asbestos
Auramine
Azsser ine
Barbituric acid, 5-othy l-5-pheny 1
Barium
Barium cyanide
Benz(c)acr idine
Benzanthrone
Benzenamine hydrochlor ide
Benzeno
Empirical
Formula
SbCI5
C15H23CI04S
As
H3As04
As205
As203
—
C17H21N3
C5H-/N304
C12H12N203
Da
C2BaN2
C17HUN
C16H10°
C6Hflf!CI
Cfi|(R
CAS Nutaber
7647-18-9
140-57-8
7440-38-2
7778-39-4
1303-28-2
1327-63-3
13322-21-4
2465-27-2
115-02-6
50-06-6
7440-39-3
543-62-1
255-51-4
82-05-3
142-04-1
71-43-2
Analysis RCRA
Type Method Method Other
ICP ~ 6010
MS-PROB SRCH
FURN-AA . — 7060
FURM-AA — 7080
FURN-AA — 7060
rURN-AA — 7060
FBI
CCMS SRCH
HPLC — -
MS-PROB SRCH
ICP — 6010
WET
MS-PROB SRCH
CCMS SRCH
II
GCMS 1624 8240
                       62

-------
Table A.I   ITD/RCRA COMPOUND DATA (Continued)
Name in Regulation
Benzene, 1 ,2-(methy lenedioxy) -4-(2-
(octy loul f iny l)propy 1)-
Benzene, dichloromethy 1-
Denzenearsonic acid
Beozenethiol
Benzidine suifate
2-Beru imidazolccarbamic acid,
1- (buty 1 carbamoy 1)-, methyl ester
Donzo (a) anthracene
Benzo(a)pyrene
Oenzo(b) f luorant'iene
Benzo(ghi)pery lene
Oenzo(j) f luoranthene
Benzo(k) f luoranthene
2,3-Benzof luorene
Benzoic a<_id
Benzoni tr i lo, 3,5-dibromo-4-hydroxy-
Empir icol
Formula
C18.,28o3s
C7II6CI2
A6ll;As03
c6"6s
C,2tl]2N2»H204S
C14!I18N2°3
Clf!M12
C20H12
C20H,2
C24"l4
C20H12
C20M12
Cl/"l4
C7H602
C7!l3N»r20
CAS Number
120-62-7
98-87-3
998-05-6
92-87-5
531-886-2
17804-35-2
56-B5-3
60-32-8
205-99-2
191-24-2
205-82-3
207-08-0
243-17-4
65-85-0
1689-84-E
Typ«
-..
MS-PROB
HPLC
CCMS
._
HPLC-UV
GCMS
(iCMS
GCMS
GCMS
GCMS
CCMS
CCMS
CCW
GCMS
sis RCRA
Method &lathod Other
H
SRCH
— ' .
1625 8270
—
—
1625 8270
1625 8270
1625 8270
1625 8270
SRCH
1625 8270
SRCH
SRCH
SRCH
                       63

-------
Tabla A.I   ITD/RCRA COMPOUND DATA (Continued)
Empirical
Nemo in Regulation Formula
(l)-Beniopyrano(3(4-b)furo(2,3-h)(l) C23H22°6
berizopyran-6(6aH)-one, 1,2,12,128-
tetr ahydro-2-a 1 pha- i sopropeny 1-6,9-
dimethoxy
p-Benzoquinone CgH/j02
Benzotri chloride CjHgClg
Benzyl alcohol CyllgQ
Benzyl chloride C-jHyCI
Bery 1 1 i urn Be ,
gamma -BIIC CgHgClg .
alpha-BHC C6H6Clp
beta-BHC ^gllgClg
delta-BIIC C6''6CI6
Biplienyl ^12*'lO
Oiphenyl, 4-nitro ^12"9^2
4,4'-Bipyridinium, 1,1 '-dimethy I-, C12"l4N2CI2
di chloride
4-Bromo-l ,2-dichlorohenzene C()lf3Cl2flr
CAS Muaber
83-79-4
106-51-4
08-07-7
100-51-6
100-44-7
7440-41-7
7440-41-7
319-84-6
319-05-7
319-86-8
32-57-4
92-93-3
1910-42-5
18282-E9-2
Anolyoio RCRA
Typo Method Hathod Other
HPLC-UV
P-POLL
MS-PROO
SRCH
MS-PROB
ICP
GCEC
GCEC
CCEC
GCEC
tiCMS
MS-PROB
—
MS-PR03
--
SRCH
SRCH H
—
SRCH II
6010
608 8080
608 8080
608 _ 6080
608 6080
1625 8270
SRCH
--
SRCH

-------
Tab to A.I   ITO/RCRA COMPOUND DATA (Continued)
Empirical
Natno in Regulation Forrculo
l-Bromo-2-chlorobenzene CgH^CIBr
l-Broroo-3- chlorobenzeno Cgll^CIBr
4-Cromo-3-chlorophenol CgH^CIBrO
2-Bromo-4-chIoropbenol C6H4CIBrO
2 -Br omo- 4 -tert- butyl phenol CjoUjgOrO
Bromoacetone CoiLBrQ
Oromodicli loromo tdane CMCI2Br
Bromome thane CH^Br
4-Bromopheny 1 phenyl ether Cj2HgBrO
Brucine ^23"26^2^4
1,3-Butadiene, 2-chloro C4"5CI
1-Butanol, 4-(buty Initroroamino)- '•B"l8^2f'2
2-Butanone ^4"o0
2-Butanono peroxide ^B"l6^4
Butyl benzyl phthalate <-]Q"20^4
2-sec-buty 1 -4 ,6-d i r. i tropbenol C in" 12^2^5
CAS Number
694-00-4
1008-37-2
13631-21-5
695-96-5
2198-66-5
690-31-2
75-27-4
74-83-9
10:-55-3
357-57-3
126-t.J-?
3tJ17-ll-6
73-63-1
1332-73-4
05-68-7
88-85-7
Ar.olyoU RCRA
Typo HothoJ Hetbod Other
CCMS
CCMS
MS-PR3B
MS-PROB
MS-PROB
MS-PROB
CCMS
CCMS
CCMS
HPLC
MS-PROB
._
CCMS
--
CCMS
CCEC
SRCH
SRCH
S^CH
SRCH
SRCH
SRCH
1624 8240
1624 8240
1625 0270
--
SRCH
—
1624 8240
II
1625 8270
615 G090
                       65

-------
Tab la A.I   ITD/RCRA COMPOUND OATA (Continuad)   .
Memo In Regulation
Cadmium
Calcium chroma te
Calcium cyanide
Calcium salt (of saccharin)
Carbamic acid, diethy Mi thio,
2-chlorual ly 1 ester
Carbamic acid, m-chloro,4-chloro-2-
butynyl ester
Carbamic acid, methyl-, 1-naphthyl
ester
Carbarr/ic acid, methyl-, 2,3-
(d i me thy 1 mo thy 1 ened i oxy) pliany 1 ester
Carbamic acid, methyl-, 2,2-dihydro-
2 ,2- dimethyl -7-benzof urany 1 ester
Carbamic acio', methyl-, 4-dimethyl-
amino-3,5~xy !y 1 ester
Carbazole
Carbon disulf ide
Carbon oxyfluoride
Eraplr icol
Formula CAS flmaber
Cd 7440-43-0
Ca«CrH204 13765-10-0
C2CaN9 EQ2-01-8
C7ll5N03S»l/2Co 6405-34-3
C8IIHCINS2 85-06-7
C11H9N02CI2 101-27-9
C12HnN02 63-25-2
formula 22781-23-3
C12H13rj°3 1563-66-2
1 ** 1 8 2 2 315-18-4
C12H9N 86-74-8
CS2 75-1B-0
CF20 3353-60-4
Anolyoio flCHA
Type Method Kathod Other
ICP — 6010
ICP — 6010 II
WET
II
CCHS SRCJ;
HPLC-UV 632
HPLC-UV 632
-_
HPLC-UV 632
IIPLC-UV 632
GCMS 1625 0270
CCUS SRCH
._
                       66

-------
Table A.I   ITD/RCRA COMPOUND DATA  (Continued)
Nam- in Regulotion
Chloral
Chlorambuci 1
Clilordane
Chlorinated benzenes, NOS
Chlorinated ethane, NOS
Chlorinated f luorocarbons, NOS
Chlorinated napthalene, NOS
Chlorinated phenol, NOS
Chlorine
l-Chloro-2,3-epoxy propane
4-Chloro-2-ni troani 1 ine
l-Chloro-3,5-dibromobenzeno
4-Chloro-3-methy Ipher.ol
l-Chloro-3-ni trobenzone
2 -Chloro-4-t-bufcy 1 phenol
6-Chloro-o-cresol
Empirical
Formulo
C2HCI30
C,4II19CI2N02
C10M6CI6
C6»6-«C'x
C2»6-xC'x
--
cio"o-xcls
c6"6-,
-------
Table A.I   ITO/KCRA COMPOUND DATA (Continued)
Home in Regulation
Ch 1 oroaceta 1 dehyda
Chloroacotoni tri le
Chloroallcylethei-s, NOS
p-Chiuroani 1 ino
Chlorobenzene
Chlorobenzi late
Chloroe thane
bis(2-Chloroothoxy)mothane
bis(2-Chloroethyl) ether
N,N-Bis(2-chloroethyl)-2-naphthylaoine
2-Chloroethy 1 vinyl ether
Chloroform
Ch 1 ore < socyanotobenzene
bi s (2-Chloroi sopropy 1) ether
Chloromethano
Chloromethy 1 methyl ether
Empirical
Formula
C2II3CIO
C2II2NCI
--
C6H6HCI
W
C16Hi4CI2°3
C2H6CI
C6H10CIV02
C4HUC!20
C14H15CI2N
C4HVCIO
CHCI3
CVH4NCIO
C6H,2CI20
CII3CI
C2!I5CIO
CAS Nuabor
107-20-0
107-14-2

108-47-8
10Q-90-7
610-16-5
75-00-3
111-01-1
111-44-4
494-02-1
110-75-0
67-66-3
51124-03-3
108-60-1
74-87-3
107-30-2
Anolyoio
Typo Hothod
--
CCMS
GCMS
CCMS
GCMS
GCE.C
CCMS
ecus
GCMS
MS-PROB
CCMS
ccys
MS-PROO
GCMS
CCMS
--
—
SRCH
—
SRCH
1624
6081
1624
1625
1625
SRCH
1624
1624
SRCH
1625
1624
--
RCRA
ttSaihod Other




8240

8240
8270
8270

8240
8240

8270
8240
II

-------
Table A.I   ITD/RCRA COMPOUND DATA (Continued)
Warns in Regulation
Bis(chloromethy 1) ether
1 - (Cli 1 orome thy 1 ) naphtha 1 one
2-Chloronaphtha*. ene
2-Clilorophenol
p-Chlorophenol
m-Chlorophcnol
1- (o-Chloropheny 1) thiouroa
4-Chlorophony Ipheny 1 ether
3-Chloropropene
?-Chloropropioni tr i le
Cholesterol
Chromium
Clirysone
Citrus red No. 2
Coal tars
Cobalt (II) chloride
Empirical
Formula
C2U4CI20
C,0l(gCI
C10M7CI
C6HbCIO
C6H5CIO
C6H6CIO
C7II,M2C'S
C,2li9CIO
C3»5CI
C3II4NCI
C27H460
Cr
CJ8"l2
C10H,6N203
--
CoCIo
CAS Numbor
6542-88-1
86-52-2
91-58-7
95-S/-8
106-48-9
108-43-0
."344-82-1
7005-72-3
107-05-1
542-76-7
57-88-5
7440-47-3
2168-01-9
6358-63-8
8007-45-2
7646-79-9
Analysis RCRA
Typo Method Method Othor
GCMS
GCMS
GCMS
GCMS
CCMS
fiCMS
GCMS
CCMS
MS-PROB
MS-PROB
GCMS
JCP
GCM5
IIPLC
CCMS
ICP
SRCH H
SRCH
1625 ' 8270
1625 8270
SRCH
SRCH
SRCH
1625 8270
SRCH
SRCH
SRCH
6010
J625 8270
--
—
6010
                       69

-------
Tcbla A.I   ITD/RCRA COMPOUND DATA (Continued)
Name in Regulation
Cobalt, when in the form of par ides
100 microns or less
Coppar
Copper cyan i do
Copper cyan i da
Coumar i n, 3-ch 1 oro-7-hydroxy-4-«sethy 1 - ,
0-aster *ith c,o-diothyl
py rophosphoroth i oste
Creosote
o-Cresol
p-Cresol
ra-Cresol
Cresols
CroLona 1 dehyde
Crotonic acid, 2- (1 -methy (hopty l)-4, 6-
Eciplrical
Formula
Co

Cu
CNCu
C2N2C«
Cg|)602


—
C,H80
C7HB0
C7»lftO
C7H80
C4"6»
C,8H2,N206
CAS Nurior
7440-48-4

7440-68-8
644-92-3
147c»3-77-0
56-72-4


8021-39-4
05-48-7
10S-44-5
103-38-4
1319-77-3
4170-30-3
3U300-45-3
Anolyoio RCRA
Type Mathod Mathod OLhsr
ICP

ICP
ICP
ICP
GC-NPD


CCMS
OCMS
CCMS
ecus
CCMS
MS-PROB
CC-PROB
6010

6010
6010
6010
622 M


SRCH
SRCH
SRCfl
SRCH
SRCH
SRCH
SRCH
  dinitrophenyI ester

Crotonic acid, 3-hydroxy, alpha-
  methyl ben/y! eftter, dinethy I
  phosphate (£)-
                         7700-17-6
CCMS
SRCH
                       70

-------
Teblo A.I   I10/RCRA COMPOUND DATA (Continued)
Name in Regulation
Crotonic acid, 3-hydroxy, methyl ester,
dimethyl photphato (E)-
Cyanides (soluble salts and
complexes) NQS
Cyanogen
Cyanogen bromide
Cyanogen chloride
Cycasin
4-Cyclohoxcne-l,2-dicarboxii!)ida N-
((1 1,1,2, 2-tetrach loroethy 1) thio) -
4-Cyclohexone-l,2-dicarboxitnide N-
(tricJilorometnyl)lnio-
2~Cyc 1 ohexy 1 -4 , 6-di n i tropheno 1
Cy cl ophospham i da
p-Cymeno
Daunornycin
4,4'-DOO
4, 4 'DDE
£jnp i r i ci? 1
Forouia
C7HI306P
—
C2H2
CNDr
CNCI
C8((16W207
C,0M5N02CI4S
C9M4N02CI35
C12HHN206
C7H15N2CI2OP
ClOH14
C27H29MO,0
C14»IOCI4
Ci4MBCI4
CAS Number
7786-34-7
52-17-5
460-19-5
G03-68-3
606-77-4
14901-08-7
2425-08-1
133-06-2
1131-89-5
50-18-0
99-87-5
20020-81-3
'2-54-8
722-56-9
Anolynii?
Type Kothod
GC-NPO
WET
—
--
—
HPLC
CC-PROB
CCEC
GC-PR08
HS-PR03
CCMS
HPLC
GCEC
CCEC
SRCH
—
--
—
--
—
SRCH
617
SRCH
SRCH
1625
--
500
608
RCRA
Mothod Other


H
II
H





8270

8080
8CQO
                       71

-------
Tebla A.I   ITD/RCRA COMPOUND DATA  (Continued)
Nacio In Regulation
4, A 'DDT
Docach 1 orob i pheny 1
n-Decane
Oi-n-butyl ph thai ate
Oi -n-propylni trosamine
2,6-di-tert-Buty l-p-benzoquinono
Dial late
2 , 6-D i aro i no to 1 uene
0 i benx (a , It) acr i d 1 ne
Dibenz(a, j)acr idina
Oiben/o(a,e)pyrena
Dibonro (a, h) anthracene
Dibinzo(a,h)pyrone
7*i -Diboruo (c , g)carba/olo
Dib«iuo( uran
Dibon/oth iophone
Esip J r i c o 1
Formula
CMllgC!5
C12CI10
C10M22
CI6"22°4
C6HHN20
CHH130
C10II|7CIKOS
C4II10N2
C21H13N
C2,H13N
C24M12
C22H,4
C24"l4
C20"!3N
C,2II80
c,2;ifls
CAS Murobor
60-29-3
2051-24-3
124-18-5
117-84-0
621-64-7
719-22-2
2303-16-4
823-40-5
226-36-8
224-42-0
182-85-4
53-70-3
.189-64-0
194-60-2
132-64-9
132-65-0
Analysis
Typo Method
GCEC
MS-PROB
ecus
CCMS
GCMS
ecus
--
GCMS
MS-PROB
MS-PROO
GCMS
CCMS
GCMS
MAS
CCMS
CCMS
COS
SRCH
1625
1626
1625
SRCH
--
SRCH
SRCIi
SRCH
SRCH
1625
SRCH
-_
1626
1625
RCRA
Method Other
8080

8270
8270
8270






8270


8270
0270
                       72

-------
Table A.I   ITO/RCRA COMPOUND DATA (Continued)
Nsmo in Regulation
1 ,2-DiOromo-3-cMoropropano
1 ,3-Dibrorcobenjena
Dibromochlorcmothano
1 ,2-DtbromooUiano
DibroraorocUiane
trans- 1 ,2-DicMoroelhcne
2,3-DicMoro-l-propanoI
trans 1 ,4-D»chl
-------
Tabla A.I   ITD/RCRA COMPOUND DATA (Cc.vtinued)
Natno in Regulation
1,4-Dichloro^enzene
1,3-Dichlorobenzeno
Dictiloroben/one, NOS
3, 3 ' -D i cli 1 oroben* i d i ne
Dicblcrodif luororoe thane
1 , 1 -D i ch 1 oroottoane
1 ,2-Dichloroethane
1, 1-Dichloroethene
cis-1 ,2-Dirhloroethylene
Dichloroothylene, NOS
2, 3-Oichloronophtha lone
2,3-Dichloroni t-robenzeiie
2,6-Oichloroplionol
2,4-Oichloroplienol
2,5-Oichlorophenol
Empirical
Forsiulo CAS Ku^bor
C6H4CI2 106-46-7
C6H,jCI2 541-73-1
C6II4CI2 25321-22-6
C12II10N2CI2 91-94-1
CCI2F2 75-71-8
C2M2CI2 75-34-3
C2H4CI2 107-06-2
C2H2CI2 7S-3S-4
C2H2CI2 156-59-2
C2H2CI2 25323-30-2
C10i:6CI2 2050-75-1
C6H3NCI202 3209-22-1
Cgl^CI^' 67-65-0
CCII4CI20 120-83-2
C6II4CI-.0 583-78-8
Anolysia
Type Method
GCMS
GCMS
GCMS
ecus
CCMS
CCMS
GCMS
CCMS
CCMS
CCMS
CCMS
GCMS
CCMS
CCMS
MS-PROB
1626
1625
—
J625
SRCH
1624
1624
1624
SRCH
—
SRCH
SRCH .
SRCH
1625
SRCH
RCHA
Method Other
8270
0270

8270

8240
8240
8240





8270


-------
                                Tablo A.I   ITO/RCRA COMPOUND DATA  (Contlnuad)
Nemo 'n Hogulotion
2,4-Dichloroplienoxyacetic acid, salts
and esters
Dichloropheiy larsino
1,2-Dichloropropane
1,3-Dichloropropane
Dichloropropane, NOS
Dichloropropanol , NOS
1,3-Oichloropropone
cis-1 ,3-Oictiloropropone
trans-1 ,3-Oichloropropene
Dichloropropene, NOS
Dioldr i n
1 , 2:3,4- Dicpoxy butane
Di ethyl other
Dicttiyl ph thai ate
0,0-Di ethyl S-methyl ester of
Empirical
Formula
cait6ci2o3
C6!l5AsCI2
C3II6CI2
C3H6CI2
C3H6CI2
C3n6ci2o
C3H4CI2
C3n4lci2
C3I(4CI2
C3M4CI2
C12H8CIS0
C4!I602
c2H6n
Cl2"H°'l
Cbll,302PS2
CAS Humbor
94-76-7
G96-28-6
78-87-6
26638-19-7
--
--
542-75-6
10061-01 -F
10061-02-6
26952-23-8
60-57-1
1464-53-5
60-29-7
84-66-2
3288-50-2
Analyoia RCRA
Type Method Method Other
GCEC
-- '
GCMS
GCMS
GCMS
GCMS
GCMS
GCMS
GCMS
GCMS
CCEC
GCMS
GCMS
CCMS
MS-PROB
615 B150 M
H
1624 8240
SRCH
. __
• •
SRCM
SRCH
SRCU
SRCH
508 8080
SRCH
1624 8240
1625 0270
SRCH
phosphorodithioic acid
                                                       75

-------
Tab Io A.I   ITO/RCRA COMPOUND DATA (Continued)
Nemo in Regulation
0-0-Diethyl-0-(2-pyrazinyl)
phosphoro th i oate
Diethy tarsine
N.N ' -0 i ethy 1 hydraz i no
0,0-Diethy Iphosphoric acid, 0-p-nitro-
phenyl ester
DieUiylsti tbesterol
1 ,3-Dt f luornbenzene
Dihydro;af role
3 , 4-D i hydroxy-a 1 pha- (methy 1 awi ;
-------
Table A.I   ITD/RCRA COMPOUND DATA (Continued)
Mama in Regulation
Dimethyl plithalato
Di methyl sulfate
Dimethyl sulfono
Dimethyl sulfoxide
3, 3-D i mo thy 1 - 1 - (ma thy 1 th io) -2-butanono-
0-[ (methyl ami no) carbonyl] oxlse
p-DimeUiy lami noazobenzono
7,12-Dimethylbenz(a)anthracene
3 , 3 ' -D i me thy 1 ben i \ J i ««
Dimcthy Icarbamoy ! chloride
N,N-Di methyl formamido
1, 1-D into thy Ihydrazine
1 , 2-D i methy 1 hy dr a z i ne
3, 6-D i methy 1 plicnan thread
2, 7-Dimethy Iphcnanthrene
a Ipha, alpha -Dime thy Iphnnsthy Icmine
Err.piricel
Formula
C10H10n4
C2II604S
C2II6502
C2M6SO
C0II20N202S
^14"i5N3
C20il16
CHH16N2
r3nr>Ncio
C3H7NO
C2ll(jN2
C2llflN2
r3G"l4
C10"14
C10''I5N
CAS Number
131-11-3
77-78-1
67-71-0
67-68-5
31916-18-4
60-11-7
57-97-6
119-93-7
79-44-7
68-12-2
57-14-7
540-73-8
1576-67-6
1576-59-8
122-09-8
Analysis RCRA
Type Method Hotltod Other
GCMS
--
GCMS
GCMS
--
GCMS
ecus
MS-PROB
—
CCMS
GCMS
CCMS
GCMS
CCMS
MS-PROB
162S 8270
II
SRCH
SRCH
—
SRCH
SRCH
SHCII
H
SRCH
SRCH
SRCH
SRCH
SRCH
SRCH
                       77

-------
Table A.I   ITD/RCRA COMPOUND DATA (Continued)
Name in Regulation
2 , *-D i TOO liiy ! p!i£f:u I
4,6-Dini tro-o-crasoi
1 , 3-D i n i Lrobenzene
f)ini trobenicr.z, KUS
2,4-Dini tropiiuiiu!
2 ,4-Dini trotoluente
2,6-Dini trotoluuno
1,4-Dioxan.e
Diphenyl •stlier
Dipheny iodine
Dip'icr.yls.Tiins, 4-nifcroso-
Oipheny Misulf ido
1 ,2-Dipheny Ihydi azino
DJSIJ! foton
2,4-Oi Lliiobi uret
n-Oocosane
Erapiricol
Formula CAS rJ'xnbor
C8H100 105-67-9
C7!I6M205 R34-B2-1
CCI!4N?°4 100-25-4
C^I^NoO^ 1-16-4
C6I!4N205 51-28-5
C7H6w204 121-14-2
C7H6N204 606-20-2
C4H802 123-01-1
C12fl100 101-84-8
Ci'/»!jN 122-39-4
C12(I10N2° 156-10-5
1. 1 o> • j ** j"7 co2""33~ /
C1?H,?N7 122-66-7
Ca!!,g02PS3 298-04-4
C2HSN3S2 541-53-7
C9otl4fi 629-97-0
Analysis
Type Hothod
CCMS
CCMS
CCMS
CCMS
CCMS
ecus
ecus
GCMS
GCMS
CCMS
GCMS
CCMS
CCMS
CCN-PO
HPLC
CCMS
1625
1525
SRCH
—
1625
1625
1625
1624
1625
1625
SRCH
SRCH
1625
622
—
1625
RCRA
Method Other
8270
8270


8270
8270
8270
8240
8270
8270


8270
8140

8270
                       78

-------
Tobla A.I   ITD/RCRA COMPOUND DATA (Continued)
. Empirical
Ncma in RoQiiletion Formula
n-Dodecane • ^-12"2£
n-Eicosane . *-"o"42
Endosul fan CgllgClgO^S
Endosul fan sulfato CgM6CI604S
Endosul fan-I C^CI^CjC
Endosulfan-II C6llgCI603S
Endrin Cj2i!8ClgO
Endrin alcohol C12l!flClgO
Endrin aldehydo -l^'a^'o-
Endrin and metabolites
Endrin ketone ^12"s-'6^
Etlianol. 2-chloro- C2I!5CIO
Ether, 2,4-dichloropheny 1 p-ni tropheny 1 - Cj'jII/NC^Oj
Ethyl carbamate CgllyNf^
Ethyl cyanide . CjllcN
Ethyl tncthacry lato ^-G"lo"2
CAS Number
1.'.2 10-3
112-S5-8
115-29-7
1031-07-8
»»y-98-8
33213-S5-9
72-20-fl
33058-12-7
7421-93-4
.
63494-70-5
107-07-3
1836-76-5
51-79-6
107-12-0
07-63-2
Anolyolo
Type Method
CCM5
GCMS
GCEC
CCEC
GCEC
GCEC
GCEC
--
GCEC
GCEC
—
MS-PROB
--
MS-PROB
MS-PROD
CCMS
1626
1625
608
608
608
608
608
--
608
608
—
SRCH
—
SRCU
SRCU
SRCU
RCRA
Uathod Other
8270
8270

8080
8080
8080
8080

8080
8080






                       79

-------
f«b!s A.I   ITD/RCRA COMPOUND DATA (Continued)
Name in Rogulotion
Ft-.hyl raethanesulfonate
<•' >yl benzene
Ethyl ene oxido (oxirane)
Ethy lenobisdi thiocarbamic acid,
salts and esters
Ethy lonebisdi thi oca rbaraic acid,
-manganese salt
Ethy lenebi.jdi thi carbamic acid,
-sodium salt
Ethy lenebi sdi thi ocarbaroic acid,
-zinc sait
Ethy icneimino
Ethy ! enoth i ourea
bis(2-Ethylhexyl) phthalete
Fluoranthene
Fluorono
Fluorine
2-Fluoroacctarr>ide
Empirical
formula CAS Number
C3Ha03S 62-50-0
CeHJO 100-41-4
C2M40 76-21-8
C4!iaN2S4 111-64-6
C4H6N2S4Mn 12427-38-2
C4H6N2S(|Na2 142-59-6
C4H5N2S4Zn 12122-67-7
C2H5N 151-56-4
C3II6N2S 96-45-7
C24H3B°4 117-81-7
C!£HIO 206-44-0
C13MU) B6-73-7
F2 7782-41-4
C9!idNFO 640-19-7
Aiialyolo RCRA
Typa Method Method Other
—
GCMS
CCMS
HPLC
CC-PROB
CS2
CS2
MAS
HPLC
GCMS
GCMS
CCMS
--
MS-PROB
H
1624 8240
SRCH
__
SRCH
630
630
—
—
1626 8270
1625 8770
1625 8270
._
SRCH
                       80

-------
                                 Table A.I   ITD/RCRA COMPOUND DATA  (Continued)
Empirical
Name in Regulation •'• formula
Fluoroacelic acid, sodium salt C'^^fQrflz
Formaldehyde CI^O
Formic acid CII202
Forsic acid, 2-(4-(5-ni tro-2-fury 1)- Cg(!6N404S
2-thiazolyl)hydrazido
(2,3,4-gt»)f'yrr°l izine-2,6(3H)dione, formula
(4,5,8,10,12,13,13a,13b-octahydro-
4 , 5-di shyoroxy-3,4,E-tr iroothy !••
2t.'-(l,6) dio-.acycloundoci'.o-
Glutarimtdo, 3-(2-(3,5-diiaethy 1-2- C15i!?3"94
oxocyc 1 ohexy 1 ) -2-hydroxyethy 1
G.'yc idyl aldehyde C3M402
Holomethars, NOS r.H3X
iioptachlor ^lo"s^'7
Ijpi/achlor epoxide ^lo"5^'7^
lleptachlor epoxide (alpha, beta, and
Anolyoio
CAS Number Typ« Method
62-7-1-8 line
50-00-0
64-18-6
3S70-76-0
3l«5-22-0
f>6-8t-9 IIPLC
765-3-S-4
1-19-3 CCMS
76-44-8 GCtC 608
1024-57-3 GCEC 603
1-19-5 GCEC 608
RCRA
. Mathod Other
II





H

8080
8080
8000
gamma isomors)
8,fla-liexahydro-l ,4:6,8-ondo,  cndo-
dinietlianonaphthatene
                                        C12H6CIG
-165-73-6
GCCC
608
3080
                                                        81

-------
Tab I« A.I   ITD/RCRA COMPOUND DATA (Continued}
Name In Regulation
Moxachlorobeiuene
Hexachlorobutadiene
Hexechlorocyctohoxane (all isooors)
Hexach 1 orocyc 1 opontad i one
Hexach 1 or odibenzo-p-di ox ins
Hexach lorodibeiizof urans
llexacliloroet.hano
Hexach 1 otophone
Hoxachloropropene
n-Moxacosano
n-Hoxadecane
Hexaethy 1 tetraphosphate
2-Hexanone
Hydantoin, 5,5-diphonyl-
Hydantoin, 5,5-diphony l-monosodium salt
Hydrazino
Empirical
Formula
V«6
C4CI6
C6'%CI6
C5CI6
C12H2CI602
C12H2CI60
C2CI6
C13H6CI602
^'6
C2GH54
C16»(34
C12!I30°13P
CC»12°
f15H12N202
Clbl(12N2°2*N8
42
CAS Kuabor
116-74-1
07-68-3
608-73-1
77-47-4
1-20-0
70-30-4
67-72-1
70-30-4
1888-71-7
6EO-01-3
644-76-3
757-50-4
591-76-6
67-41-0
630-93-3
302-01-2
Analysis RCRA
Type L'othodl CJIetihod Other
CCMS
CCWS
GCEC
CCMS
CLP
CLP
CCMS
HPLC
MS-PROS
CCMS
CCMS
HPLC
ecus
GCMS
—
HPLC
1625 8270
1625 8270
608 8000
1625 6270
—
—
1625 B270
H
SRCH
1625 8270
1625 8270
—
SRCH
SRCH
—
..

-------
Tub)a A.i   ITD/RCRA COMPOUND DATA (Continuod)
Norao >n Regulation
Hydrocyanic acid
Hydrofluoric acid
Hydrogen sulfide
Hydroquinona
Hydroxydimelhy Inrsine oxido
N- (2-hydroxy ethyl) ethyl enoimi no
Hydroxyalmine, N-ni troso-N-pheny I-,
ammonium salt
Hyf.ochlorous acid, calcium salt
Hypochlorous acid, sodium salt
2-lm\>ii\zo\ idinono, l-(5-ni tro-2-
thiazoly 1)-
Indeno(l ,2,3-cd)pyreno
lodomotliano
Iron-doxtran complex
Isobutyl alcohol
Isocyanic acid, methyl oster
Empirical
Formula
Cl IN
(IF
H2S
C6II602
C2ll7Ar,02
C4H9NO
C6H6M202«H3M
CI202Ca
ClOHa
C6M6M403S
C22H]2
CII3I
Unknown
C4H100
C2!I3NO
CAS Wurabor
74-90-8
7664-39-3
7763-06-4
123-31-9
75-60-6
1072-52-2
135-20-6
7770-54-3
7681-52-9
61-57-4
193-39-5
74-88-5
9004-66-4
78-03- J
624-83-9
Anolycio RCRA
Typo ilQthod tioifiod Other
• -- .
WET
WET
_.
HPLC
HPLC
(IFLC
1VET — II
H
HPLC
CCMS 1G25 8270
CCMS SRCH
ICP — 6010
CCMS , SRCH
II
                       83

-------
Toble A.I   ITD/RCRA COMPOUND DATA (Continued)
Name In Regulation
Isonicotinic acid hydrazido
IsopSorone
2-Isopropy 1 naphtha 1 one
Isosafroii)
Kopono
Kclene
Lastocarpine
Lead
Load acetate
Lead phobpliate
Load subacetatu
L i Lh i uifl
Longi felons
Ma laic anhydride
Ualeic hydrazide
Malononi tr t le
Empirical
Forraule
C6M,N30
C9H140
C13"l4
C10li10°2
C10!IJ00
C2fl20
C21»33°7
Pb
C4l!604Pb
04P2Pb
C4n,0n0pb3
Li
' C15'»24
C4»2°3
C4II4«202
GJUN9
CAS Nuaiber
64-85-3
78-59-1
2027-17-0
120-58-1
143-bO-O
463-R1-4
303-34-4
7439-02-1
301-04-2
7446-27-7
1335-32-6
7439-93-2
476-20-7
108-31-6
123-33-1
103-77-3
AnalyaU RCRA
Typo Method Usthorf Ochor
-.
-„
GCMS SRCH
ya-PROB SRCH
US-PRQB SRCH
--
HPLC
FURN-AA — 7421
FURN-AA -- 7421
FURW-AA — 74?1
FUf.iN-AA -- 7421
ICP — 6010
CCMS SRCH
II
IIPLC
MS-PROB SRCH

-------
                                Table A.I   ITD/RCRA COMPOUND DATA  (Continued)
Name in Regulation
kielphalan
Mercury '
Mercury fulminate
Uothacry looi tri le
Mothanethiol
Methapyr i lone
1,3,4-Motheno-lH-cyclobutafcd)
pentalene, i , Ja, 2,2,3 ,3a, 4,6,5, 5a,
5b,6,-dodecachlorooctahydro-
Motliomyl
Mothcxychlor
Methyl hydrazine
Methyl mothacry late
Methyl mothonesul fonate
Methyl pa rath ion
2-Mothy 1 -2- (me thy 1 thio)propion-
E/np i r i c o 1
Foraiulo
C13H!8N2CI2°2
Hg
C2N202Hg
C4H5N
CH4S
C14HigN3S
C10CI12
C5H10N202S
C16l!15Cl3°?
CII4H2
C6"e°2
C2I!6035
Cell10fW5PS '
C7HUN20?S
CAS Number
140-82-3
7430-97-6
628-GS-4
126-98-7
74-93-1
91-80-5
2385-65-5
16752-77-5
72-43-6
60-34-4
80-62-6
66-27-3
298-00-0
116-06-3
Analysis
Typo Method
HPLC
CV-AA
CV-AA
MAS
GCMS
GCMS
CCEC
HPLC-UY
CCEC
ItPLC
CCMS
MS-PROB
GC-NPO
CC-PROB
._
—
.__
SRCH
SRCH
SRCH
617
632
608
--
SRCH
SRCH
672
SRCH
RCRA
Method Other

7440
7440





8080





aldchyde-0-(raethyIcarbonyI) oxime

-------
Tablo K.I   ITD/RCRA COMPOUND DATA (Contlnuod)  .
tapir ica!
Nniao in Regulation Formula
4-Methy 1 -2-pentanone CgHj^O
M-Uethyl-N'-ni tro-N-Ni trosoguaoidino ^"s^S^S
2-Mothy \aiir idine £3"^
2-Metbylben/otliioa/olo Cgll/NS
WeUiy Ichlorocarbonate C2li;jCI02
3-Mothy Icholanthrene . ^2l"i6
Hethyleno chloride CH2CI2
4,5-Mothy lone pfienanthrene ^lb"lO
4,4'-yotliy lono-bis(2-chlorooni 1 ino) ^13")'>'-'2^2
4 Mot'iy 1 fluorene ^H*'l2
1-Methylf luorcne M4f'i2
2-Wott.yllactonitri le C^H/NO
2-Methy 1 n.iplitha lono ^il'(10
1-Uothy IpKunanthrene ^Ib"l2
9-MoUiy Iplionantlvi er.o ^!5")2
2-(iyiothylLhio)bonzoUiia2ole C^i/ffS.^
CAS f-Jtobor
108-10-1
70-25-7
76-65-8
120-76-2
79-22-1
66-J0-5
'76-09-2
203-64-5
101-14-4
155C-99-S
1730-37-6
/5-M-6
91-57-6
032-63-9
083-20-6
615-22-6
Anolyols RCPA
Typo Llotliod Mclhcdl Older
CCMS
W'LC
MAS
CCMS
—
CCMS
CCMS
CCMS
CCMS
CCMS
CCMS
...
ecus
ecus
CCMS
CCMS
SRCH
—
SSCH
SRCH
__
SRCH
1624 82-10
SRCH
SRCH
SRCH
SRCH
H
SRCH
SRCH
SRCH
SRCH

-------
TobloA.J   ITD/RCRA COLSPOUXD DATA  (Continuod)
fJoa!o in Regulation
Uolhy 1 tli i otirac i (o
Mustard gas
Naphthalene
1 .S-Njplilhslenediamine
1 , 4 -Napl.lliocjutDorio
1 , 4 -Wapiitlioqu i (tone, 2, 3-di ch 1 or o-
l-Naplitliyl-2-Uiiour«a
boto-N.iplit.liy 1 ami no
1-Haphtliy laaine
Nickel
Nickel carbemyl
Nickol cyanide
Kicotino and salts, NOS
Nicotine oxoiate
Nitric oxide
Nitrites
Erapiricol
Foraulo CAS Hirr&er
C6!I6N2OS 56-04-2
C4flaCI2S 605-60-2
CJ0lla 91-20-3
C10MIOM2 2243-C2-1
C101I602 130-16-4
Ca"4CI2°2 117-80-6
Cll"lON2S 86-eO-»
C10/igp; oi-59-e
C|(yi^< 134-32-7
Hi 7440-C2-0
C404Ni 13463-39-3
C?N2Ni 5S/-19-7
<",0II14H2 54-11-5
C,0il,4N2»KC2l)204 23r58-42-l
NO 10102-43-0
H797-G5-0
Anolyaia RCRA
Typo Method tlolhod Other
KPLC
M
CCMS 1625 0270
WS-PROB SRCH
us-pnoo sncn
CC-PROO SRCil
IIPLC
CCMS 1625 0270
CCUS SRCH
ICP -- 6010
ICP -- 6010
ICP — 6010
MS -PROD SRCIi
It
..
Rt?

-------
To&ta A.t   ITO/RCflA CCWPKBSO BATA
Ec^irtcai
Mono In Regulation Foreulo
5-Nitro-o-toluidina *-7"e^2"2
2-Ni troani 1 ine ^&^6^2^2
3-Nitroani 1 ine CgHcN^Oo
p-Ni troani 1 ine Cgtlgf^f^
Nitrobenzene Cgligiii^
Nitrogen dioxide MQ2
Nitrogen mustard C^H^jC^N
Nitrogen mustard and hydrochlorida salt CgHj2f '3N
Nitrogen mustard N-oxide CgH||CI2NQ
Nitrogen mustard N-oxide, hydro- Cglli2CI3NO
chloride salt
Nitroglycerin C3HgM3Qg
2-Ni t roplieno 1 CgHgN03
4-Nitroptienol CgMgt^
4-Nitroquinol ihe-1-oxide ^Q^6^2^3
Ni trossmine, NOS
CAS Minsbor
09-55-3
flS-74-fl
80-09-2
100-01 -6
90-95-3
10102-4^-0
51-75-2
1-26-2
126-35-2
302-70-5
B5-63-0
88-7S-5
100-02-7
B8-67-5
35578-91-1
Analysis
Typo Method
GCMS
.CCMS
CCMS
ecus
ocys
—
—
—
MS-PROB
--
MAS
GCMS
ccys
CCMS
_.
SRCH
SRCH
SRCH
SRCH
1625
—
_.
—
SRCH
--
SRCH
162S
1625
SRCH
__
RCRA
Method Other




8270
II
II
H

H

8270
8270


                       88

-------
Tab I o A.I    ITD/RCRA CDfiPCU?iD DATA  (Continued)
Nama in Regulation
N-Ni troso-N-othy 1 urea
N-N i troso-N-methy I urea
N-Ni troso-N-methy 1 urethana
1 N-N i trosod i -n-bu ty 1 ami ne
N-Ni trosod i ethano 1 ami ne
N-N i trosod i ethy 1 ami ne
N-Ni trosod imethy famine
N-N i trosod i phe ty 1 an i ne
N-N i trosomethy 1 ethy 1 ami no
N-N i trosomethy 1 pheny 1 ami na
N-N i trosomethy 1 y i ny 1 ami ne
N-Nitrosomorphol ine
N-Ni trosonorni co tine
N-N i trosop i per i d i ne
N-Wi trososarcosino
Empirical
For c?,u 1 a
C3H7N302
C2HSN302
C4HBN203
C8H10N20
4 1(^2 3
C *Ht iy»2"
C2H6N20
C12H10N20
C3H8N20
C7H0N20
C3H6N20
C4H8N202
C9"llN30
C5II10N20
C3H6N203
CAS Nuabor
76S-73-9
684-93-5
615-53-2
024-IS-3
1HS-S4-7
S5-18-6
62-75-9
Bo-30-6
10595-95-6
£14-00-6
4S49-40-0
B9-8S-2
16533-55-8
100-76-4
132B6-22-9
Ann! pole RCRA
Typo Hothod Wothoc! Other
HPLC
JfLC
J1PLC
CCHS SRCH
HPLC
GCMS SRCH
GCMS 1325 8270
GCMS 1625 8270
GCMS SRCH
GCMS SRCH
HPLC
HPLC
ItPLC
MS-PROD SRCH
HPLC

-------
fab Ia * 1   ITD/RCRA COMPOUND DATA (Continued)
Nama in Regulation
17-alpha-19-Norpregnp-l,3,6(10)-
trien-20-yn-17-OI, 3-methoxy-
n-Octacosane
n-Octadecane
OctaraethylpyrpphosphoraEiide
Osmiura totroxide
7-Oxal)icyclo[2.2.1]heptane-2,3-
iiicarboxyl ic acid
2-Oxetanone
4,4'-Oxydiani 1 ine
Paraldehyde
Parathion
PCB-1016
PCB-1221
PCB-1232
PCB-1242
PCB-1248
Ewpiricnl
Fornufo CAS fcalbor
C21fl26°2 72-33-3
C28H58 830-02-4
C18U38 593-45-3
C8H24N4°3P2 152-16-9
040s 20816-12-0
C8H1005 145-73-3
C3H402 57-57-8
c12n14M2o ioi-eo-4
C6Hi203 123-63-7
C10H14N05PS B6-38-2
. 12674-H-2
11104-28-2
11141-16-6
63460-21-9
12672-20-6
Analyst o
Typo Kothod
MS-PROB
COSS
CCMS
HPLC
KP
CC-PROB
MS-PROB
—
—
CCNPD
CCEC
CCEC,
CCEC
CCEC
CCEC
SRCfJ
162S
1625
—
—
SRCH
SRCH
—
--
614
60S
608
608
603
608
(2C3A
Method

8270
8270

6010




8140
8030
6080
8080
8080
8080
Other






II
. II
II







-------
                                 Table A.I   ITD/RCRA C063POUMD  DATA (Continued)
Namo in Regulation
PCB-1254
PCD- 1260
Pentaclilorobenzene
Pen.tach 1 orod i benzo-p-d i ox i ns
Pentach 1 orod ibunzofurans
Pentach 1 oroe thane
Pentach 1 oron i trobenzeno
Pentoch 1 orophono 1
Pentaf luorobenzene
Pentaf luorobromobenzeno
PentatneUiy 1 benzene
Peroxyacetic acid
Pory lone
Phenacetin
Phenanthrene
Phono 1
Enpirkol
Forcuilo CAS fJualbor
11097-69-1
11006-82-5
C6!ICI5 603-03-5
C,2H302CI5 1-28-9
Cj2H3OCI5 1-29-0
C^fClg 76-01-7
C6N02CI5 82-68-8
C6HOCI5 87-8S-5
C6»!F5 363-72-4
C6BrF6 344-04-7
C||H16 700-12-9
C2H^03 79-21-0
2^ 12 1U8-55-0
Cj()H|3N02 62-44-2
^14^10 85-01-8
Cgi'jO 108-95-2
Ana lye ie RCRA
lypo MothoJ Mothod Other
GCEC
CCEC
MS-PROB
OIOXIN
DIOXIN
GCMS
CCEC
CCMS
MS-PROB
MS-PROB
CCMS
--
GCMS
MS-PROB
GCMS
cans
608 8000
608 8080
SRCH
CLP 8280
CLP 8280
SRCH
617
1625 8270
SRCH
SRCH
SRCH
H
SRCH
SRCH
1625 8270
1625 0270
                                                         01
43l^^

-------
                                             T«blo A.I    ITD/RCRA CG!3POUH® DATA (Continued)
t&».*i*'Mi:
Mama in Ragulotlcn
Phenqthiazine
Pheny 1 ened i am i ne
o-Pheny 1 ened i ami ne
P-Pheny 1 ened i am i ne
in-Phony 1 ened i am i ne
o-Pheny 1 ened i ami ne, 4-chloro-
ra-Pheny 1 ened i ami ne, 4-methoxy- , su 1 i ota
Pheny (mercury acetate
1 -Pheny Injphthalene
2-Pheny.l naphtha 1 eno
N-Pheny 1 th i ourea
Phosgene
Phosphine
Phosphoramidothioic acid, acetatnidoy 1 ,
Q,0-bis(p~chlorophenyl) ester
Phosphoric acid, (2,2,2-trichloro-l-
hydroxyelhyl)-, dimethyl ester


	 , ... ....
Empirical
Formula
CgH7NOS
C6H8N2
CGH8N2
C6H8N2
C6H8N2
C6H7N2CI
C7H12N205S
CflHaHg02
C16»12
C16H12
C7II8W2S
cc»2o
H3P
C14»13C«2N2°2PS
C4ii8o4ci3p



CAS Huabor
92-84-2
1-29-6
' 05-54-5
106-50-3
108-45-2
65-83-0
39156-41-7
62-38-4
605-02-7
812-94-2
1103-85-5
75-44-5
7B03-61-2
4104-14-7
52-68-6

92

Analysis
Type ttathod
GCMS
—
MS-PROb
GCMS
MS-PROB
GCMS
CV-AA
GCMS
GCMS
IIPLC
—
WET
MS-PROB
GC-PROB



SRCH
—
SRCH
SRCH
SRCH
SRCH
.«
SRCI;
SRCH
"
"
--
SRCH
SRCH



RCRA
Method Othor

j
-i
I
1
i
^
•j
i

H
7440



II





'

V
1

1
• i
.'1
.i!
•4
1
. ,1
<'•
^1
i
;|
. . . • J.
. % * • . 'x

-------
                                  Table A.I   ITD/RCRA COHPCUWD DATA (Continued)
          Nemo in Regulation
Empirical                         Analysis            RCRA
 Formula         CAS PJuabsr    Typa     Eflafr.hod        Method
Phosphoric acid, l,2-dibromo-2,2-
  dichloroethyl dimethyl ester

Phosphoric acid, 2,2-dichlorovinyI
  dimethyl este-

Phosphoric acid, 2-chloro-l-(2,4,5-
  trichlorophenyl)vinyI dimethyl ester

Phosphoric acid, 2-chloro-l-2(2,4-
  dichlorophenyl)vinyl dimethyl ester

Phosphoric acid, dimethyl ester, estor
  with (E)-3-hydroxy-N,N- dimethyl-
  crotonamido

Phosphoric acid, dimethyl ester, ester
  with (E)-3-hydro«y-N-
  methylcrotonamide

Phosphoric acid, dimethyl ester, ester
  with 2-chloro-N-N-diethyl- 3-
  hydroxycrotonamido

Phosphoric acid, tri-o-tolyl ester

Phosphoric acid, trimethyl ester

Phosphoric, acid, hexamethyl-
C4H703CI2P


C10H903CI4P


C10H10°3C'3P
C7H14N05P



C10"i9N05C«P


C2lll^04P
                   300-76-5    GC-NPD    622


                    62-73-7    CC-NPO    62?


                   911-11-5    GC-HPD    622


                   470-90-6    GC-PROB   SRCH


                   141-66-2    GC-PROB   SRCS



                  6923-22-4    GC-PROB   SRCH



                 1317J-21-6    CC-PROB   SRCH



                    78-36-8    MS-PROQ   SRCH

                   B12-b6-l    MS-PROB   SRCH

                   630-31-9    GCMS      SRCH
                                                         03
                                                                 Other
                                                                                     I  *\J
                                                                                     I  -I
                                                                                    i  .-2:
il
                                                                                                                               ;.

-------
                                   Tobla A.I   ITD/RCRA COBPCIJHO DATA  (Continusd)
                in Regulation
                                           Foroulo
CAS
   Analysis)
Typo     Method
Phosphorodi thioic acid,  0,0-diethyl
  ester, S-ester with  3-(morc£ipto-
  iaothyl)-l,2,3-bocuotria2in-4(3H)-one

Phosphorodi thioic acid,  Q-0-diethyf
  0-(2-(ethylthiu)ethyi)  astar  misted
'  with 0,0-diethyl S-(2-(ethylthio)
  ethyl) ester  (7:3)

Phosphorodi thioic acid,  0,0-diethyl
  0- (2- i sopropy I -6-Biothy I -4-
  pyriraidinyl) ester

Phosphorodi thioic acid,  0,0-diothyl
  0-(3,5,6-trichloib-?-pryidyl) ester

Phosphorodi thioic acid,  0,0-diethyl
  0-(p-(methycul f iny I) phony I  ester

Phosphorodi thioic acid,  0,0-diethyl
  S- [ (ethy I thio) methyl]  ester (phorate)

Phosphorodi thioic acid,  0,0-diethyl-
  S-[(l , i-dimethy (athyi)th(o] mo thy I
  ester

Phosphorodi thioic acid,  0,0-dimethy I
  ester, S-cster with  3-(mercaptomothy I)-
  1 , 2, 3-benzotr i az i n-4 (3H) -one
                                                            2642-71-9    GC-PROB   SRCH
                                                            8065-48-3    GC-NPO    622
                                                             333-41-5    CC-MPO    622
                                          clo"uN03C3PS
2921-63-2
116-80-2
298-02-2
13071-79-8
GC-NPD
CC-NPO
GC-NPD
,,
622
622
622
»
                                                              86-50-0    GC-NPO    622
                                                          94
Othor
**«'i^^**'«'i^^^^Xaj^^

-------


1
i ^
t *
1 "
Tub la A.I ITD/RCRA COMPOUND DATA (Continued) :
i
Name in Regulation
Phosphorodi thioic acid, 0,0-disiothyl
ester, S-ester with N-(morcaptomothyf)
phthalimide
Phosphorodi thioic acid, 0.0-dimethyl-,
0-(4-meththio)-ro-toly 1) ester
Phosphorodi thioic acid,s(((p-chloro-
pheny 1 {-hi o) methyl) 0,0-diethyl estor
Phosphorodi thioic acid, S,S'-mothylen»
0,0,0',0'-tetraethyl esfcnr
Phosphorodi thioic acid, S.S'-p-dioxono-
2,3-dryl 0,0,0',0'-tetraethyl ester
Phosphorodi thioic acid, S-(2-(ethyl-
sulf inyl)ethyl) 0,0-dimethyl ester
Phosphorothioic acid, 0,0-diroethyl
0-[p-[(ddimethy lamino)sul fony 1)
phenyl] ester
Phosphorothioic acid, phenyl, 0-(4-
bromo-2,5-dichlorophenyl)
0-methyl ester
Phosphorothioic acid, phenyl-, 0-ethyl
0-(p-ni tropheny 1) estor
Phthalic acid esters, KOS


Eoplricel
Forrculo CAS Wuinbor
C11H12N04PS2 732-11-6
c10Jilso3PS2 Bs-an-9
C11H16°2PS3 766-19-6
C9H22°4P2S4 563-12-2
C12H26°6P2S4 78-34-2
C6M15°452P 301-12-2
C10H16N05PS2 52-85-7
C13"lO°2CI2BrpS 21609-90-5
CHHHN02PS 2104-64-5
1-30-3

95
•tnwrvmaauiclMMi&jMbUfliiiUa&.a^'i ''^^-'^
CC-NPD 614 8140 \ •
.]
CC-NPD 701
•/
CC«S SRCH j
CC-PROB SRCH ! 'j
!|
"" ""* $
•I
.* -* ! ';,
*.*•!
' 'i
GCMS « |
,c!
A
\
•'•• * •-•*,, <- iy,
" ' 	 . ~: T -.'," • -t;

-------
                                                                                                 n
Table A.I   1TO/RCRA COHfGUf® DATA  (Continued)
Empirical
Name in Regulation Forctuhi
Phthalic anhydride Cgll^03
2-Picoline C8H?N
Polybroeiinated biphenyls, NOS
Polycdlorinated bi phony), NOS
Polychlorinated biphenyl, NOS
Potass Jura cyanide CNK
Potassium silver cyanide C2N2AgX
Pronaraide CjoHjjK!JOCi2 •
1,3-Propane sulfone C3Hg03S
2-Propanone C3MgO
Propionitri le, 2-hydroxy- C3llgNO
n-Propylamine ^3^9^
2-Propyn-l-ol C3H^O
Pyrene C16H10
Pyridine CgHgH

lBtttii>iBt^^»iffi»?ia»Saa2ii^<£ai»afa^»ie-a^^ i^.£l;;it -'luS"''"
CAS ^uGsfooir
85-44-9
109-OS-8
59533-65-1
1-30-0
133S-3S-3
151-50-8
503-61 -6
23050-58-5
1120-71-4
67-64-1
78-97-7
107-10-8
107-19-7
129-00-0
110-86-1
96
.„,..,,..._. •
Anolyola RCRA
Typo Mothod Hothod Other
« II
GCMS 1625 8270
CCMS SRCH
GCEC 608 8080
GCEC 608 8080
ffET
ICP — 6010
GCMS SRCH
II
GCMS If 24 8240
—
MAS SRCH
MAS SRCH
GCUS 1625 8270
MS-PR'JB SRCH

*""*" ' ""' ' -*>»'-'-A-'"-'»p«(
                                                                                                !
                                                                                                 l

-------
Tab lo A.I ITD/RCftA COMPOUND DATA (Continued)
Nome in Regulation
Pyridino, 2,6-diamino-3-(phony lazo)-,
monohydroclt 1 or i do
Pyridino, 3-chloroifiethyl-,
hydrochior ide
Reserpine
Resorcinol
Saccharin and salts
Safrole
Sal icylani 1 ide, 2'5-dichloro-4'-nitro,
compound with 2-arcinoethano! (1:1)
Solenious acid
So 1 en i um
Selenium sulfide (SaS)
Selenium sulfide (SeS2)
Solenourea
Semi carbaz ide
Silver

*bi Oft^i»ri^'iV^^u\Ml^tJL.>^»V^!:£i,&£ittBJa'fr' s'rtV-r'pv^^ti^ia^uatx't
Eopirkai
Formula
C12H12N6CI
C6H7NCI2
C33H4oN209
C7H5N03S
C10*J10°2
C16H14N305CI2
H203Se
Se
SSe
S2So
CH4N2So
CH5N30
Ag


CAS Munib®r
13S-40-3
6959-48-4
50-55-5
100-46-3
81-07-2
04-59-7
14200-40-8
7783-00-8
7782-49-2
7446-34-6
7488-56-4
630-10-4
57-56-7
7440-22-4
97
dU^^-'in^-U-' ji-VrW^A:.
Anoiyoia . ROiA
Type: Method KathorS Othar
-- H
-- H
HPLC-IV —
HPLC''\ —
ItPLC
MS-PROB SRCH
MS-PROB SRCH
( ':
f -p
\ ,
")
1
;]
';'
^
1
1
' '
FWN-AA -- 7740 1 '•
i _jj
FURN-AA -- 7740 ' ; j
ft
FUflN-AA — 7740 ! 1
FURW-AA -- 7740 j -\
i ^
FURN-AA — 7740 { .•*
'-I
i '-•'i
ICP — 6010 '
•
• ' '. |
f-4JUi*itJi^^jiwLki^Jhfti^iwj>— .•*^
. *.
-. .\
• i
>i
•J
i^.

-------
Table A.I   ITD/RCRA CflSPOUSD DATA  (Continued)
Empirical
Noraa in Regulation Formula
Silver cyanide AgCN
Sodium cyanide MaCN
Sodium salt, dihydrate (of saccharin) CyllfcNt^S^^O'
Equal ene C3(flsQ
Streptozotocin ^8"l5^3^7
Strontium sulfide SSr
Strychnine and salts ^21^22^2^2
: Styrene ^gHg
' < Succinic acid, mercapto-, di ethyl ^10^19^6^^2
ester, S-ostor with 0,0-di methyl
phosphorod i th i oa te
Sulfuric acid, di ethyl ester C^H^O^S
alpha-Terpineol ^lo"
Tetrachloroethene ^-2^4
1,2,4,5-Tetrachlorobenzene CgH2CI4
1.,2,3,4-Tetrachlorobenzene ^6^2^-'4
1 ,2,3,5-Tetrachlorobonzene CgH2CI4


WtiAiiliiui&ii^^^
CAS Wusljar
EOS-64-9
143-33-9
•No 6165-67-3
7683-64-9
. 18883-66-4
1314-96-1
57-24-9
100-42-5
121-75-5
64-67-5
98-55-5
127-1B-4
95-84-3
634-66-2
634-90-2
98

.,; , . ,.-.. .
Anslyoio RCRA
Type Method Method Other
ICP
WET
CCHS
HPLC
ICP
GCMS
GCMS
PEST
~
GCMS
GCMS
GCMS
GCMS
GCMS

	 „. _
6010
—
SRCH
—
6010
SRCH
1625 8270
614 8140
H
1625 8270
1624 8240
SRCH
SRCH
SRCH

i
"* ' «-«;•*•—. — •— — -- - - ..... .. ... — • -, ***„ ._ •^n.^- »-<-.. .^^.,.y. „».,,_„ »„, ^.i ,i 	 ••. •- ^.
V
•
:
t '"
s
••}
'• ,1
\l
• .
,(
-']

1
.;
1

|
.1
1

-------
I
!
I . ' Table
i
I

1 . •• •

Nemo in Regu'ntion
2,3,7, 8-Tetrach 1 orod i benzo-p-d i ox i n
Tetrach 1 orod i benzo-p-d i ox i ns
Tetrach 1 orod i benzof urans

1,1, 2 ,2-Tetrachl oroethane
1 , I , 1 ,2-Tetrach 1 oroethane
Tetrachloroethano, NOS
Totracli lor one thane •
2,3,5,6-Tetrachloroni trol>onzene
2,3,4,6-Tetrachlorophenrl
2,3,5,6-Tetrs«chlorophenol
2,3,4, 5-Tetrach 1 oropheno 1
n-Tetracosane
' pi
n-Tetradecane
Tetraefchyl lead

Tetraethy 1 d i th i opyrophosphate
Tetraethy ipyrophosphdte

\ ' • ' ' . ' ' ' '•
••'*>•. '.
1 • ' • \ '
'•• \ •
'•'.-. \
BwflliiBBBii*ff&ii't < n rail t-^sS&^^.^i^i^^A^^.'i'S^^Mj^S&i^^iia^^^^


A.I ITD/RCRA




Empirical
Formula
C12n4ci4o2
C12H4CI402
r n c(40

C2H2CI4
C2H2CI4
C2H2CI4
CCI4
C6IIN02C<4
C6H2OCI4
C6H2OCI4
C6H2OCI4
C24H50

C14U30
C8H20Pb

C8H20°5P2S2
C8H2007P2








fWOUND DATA






(Continued)











'1
1
:i
t
4
-»
i
Analysis RCRA •{
CAS dumber
1746-01-6
1-33-1
1-33-2

79-34-5
630-30-6
25322-20-7
S6-23-5
117-18-0
53-90-2
035-95-5
4901-51-3
648-31-1

623-59-4
78-00-2

3689-24-5
107-49-3

99




-j&J&&&^^£*i£^*^^
Tyss
OIUXIN
DIOXIN
DIOXIN

GCMS
GCMS
GCMS
GCMS
MS-PROB
GCMS
GCMS
GCMS
GCMS

GCMS
FURN-AA

GC-PROO
HPLC






Method Ue'-.hod Other
613 8280
\
'4
i •
•1
CLP 8280 P
CLP 8280 i I
I »
1624 8240
SRCH
SRCH
1624 8240
SRCH
;]
,"i
\
\
\
1
SRCH ;S
SRCH . ; I
SRC-I j^
1625 8270 i }
\ ''
1625 8270 I 5
7421 1
) "',
SRCH j i.|
H






' i
i
4
3
1
.y<

^
:j
••' • '.'•'.. .. • -jt''V-V" ' " '.'ij ''V^'li'1 '^{k*'"i"'i'v|
-2k:»Jkt^J~^,-'»i-iw^4otvV:^:Jwi^iSiiiiii*!i^ ^l^iJ^j^if»CiSSiisiisJi»^iijtA

-------
Tcblo A.I   ITD/RCRA COMPOUND DATA (Continued)
Namo in Regulation
Tetramethy 1 lead
Tetran i tromethane
Tha 1 1 i c ox i de
Tha 1 1 i urn
Tha 1 1 i urn se 1 en i to
Thai 1 ium(I)acetato
Thai 1 ium(I)carbonate
Thai 1 ium(I)cMoride
Thai 1 ium(I)ni trate
Thai 1 ium(I)sulfate
Thianaphthene ,
Thioacetamide
Thiosemicarbazide
Thiourea
Thioxanthen-9-one
Thiram

-:^';&;,i^ :;-: -:.*> .'•>.•&*:. ; .^M^.-MJ&J, a<^? .,,>:
Empirical
Formu 1 a
C4HJ2Pb
CN408
03TI2
Tl
SeTI
C2H402»TI
C03TI2
LIT!
N03TI
04STI2
CaH6S
. C2H5NS
CH5N3S
CH2N2S
C13»8°5
C6H12N2S4

.••;*v -.•;•!. ~^-y\.'.-i:-".
CAS Mumbor
7S-74-1
609-14-8
1314-32-5
7440-28-0
12039-52-0
563-68-8
6533-73-fi
7791-12-0
10102-45-1
10031-69-1
95-15-8
62-65-1
79-19-6
62-56-68
492-22-8
137-26-8
100

Analysis
Type . Method
FURN-AA —
__
ICP
FURN-AA —
FURN-AA ~
FURN-AA —
FURN-AA -
FURN-AA --
FURN-AA —
FURN-AA —
GCMS SRCH
_.
HPLC
HPLC
CCMS SRCH
CS2 630

»•'** VV'i .i^.n-<.-«rtV *"-•«„
RCRA
Mothod Other
7421

6010
7841
7841
7841
7841
7841
7841
7841

H





.••j-isT.i-tvr' • • »•

-------
                                                Table A.I   ITD/RQU COMPOUND DATA  (Continued)
 |,
«\
timss&teM;^':^,
Nemo in Regulation
Toluene
Toluene diamine
'> Toluene, 2,4-dinmino-
\ • ;
3 , 4 -To 1 uened i am i no
o-V^luidine
\
V
o-Tolu<.dino hydrochloride
\
o-Toluidme, 4-(o-toly IBZO)-
o-To 1 u i d i no ;\5-ch 1 oro-
\
p-Toluidine, atpha, alpha, alpha-
trif 1 uoro-2.6-iJ.ini tro-N,W-dipropy 1 -
p-Toluidino, N-(2-ciSloroelhy l)-2,6-
dinitro-N-propyl-afpha, alpha,
. alp!ia-tr if luoro-
\
Tolyleno Oi isocyanate \
\
Total xy lanes
Toxajjliene
n-Triacontano .

\ •
\ . •
. ErcpiricoJ
Forraula
C7Ha
Cy *"i/y*2
7102
Witfh
C7II10KCI
C7H0NCI
Cl3»I6W3
C9H6N202
C8»10
C10H,0Clfl
C30II62


CAS Mtrabar
108-68-3
25376-4B-3
65-80-7
496-72-0
05-53-4
636-21-5
97-50-3
95-70-4
15B2-09-8
33245-39-5
26471-62-5
3-25-0
E001-35-2
638-BQ-3
101

Analyolo RCRA
Typa Uothod Mothod Other
CCMS 1624 8240
—
GCfcSS SRCH
OCMS SRCH
MS-PROB SRCH
MS-PROB SRCH
MS-PROb SRCH
MS-PROO SRCH
CCEC 617
II
CCUS SRCH
CCrC 608 8060
CCMS 1625 0270

i, . .,

-------
[*-. •
y
Table
Mams In Regulation
Tri ozone, 3,3-diraethyJ-l-(p-ch!oro-
phonyl)-
S-Triazine, 2,4-dichloro-6-(o-chloro-
ani liin
Trihroiaoaia thane
1 , 1 , 2-Tr i ch loro-2-f 1 uorosthana
1,2,3-Trichlorobanzone
1,3,5-Trichlorobanzena
1,2,4-Trichlorobenzena
1,1,1-Tr icMorcethane
1,1, 2-Tr icMoroathana
ji Trichloroetheno
Trichloromethanothiol
1 Trichloromonof luoromethone
\ 2,4,6-Trichlorophenol
a 2,4,5-Trichlorophenol
^- 2,3,6-TrichJoropbenol
1
'» • .:


K.I ITO/ROSA CO&Ot&D DATA {Continued)



Ecpirif.sl Anajyolo RCRA
FcrauJo CAS tafrfjstr Typo tbthod doihod Other
C6Hi0CIM3 7203-BO-O
C^%M3C3 101-05-3 GC-PRQ8
CHBr3 75-25-2 CCMS
C2H2CI3F 369-28-4 GCtiS
C6H3CI3 87-81 -S CCfcSS
CG^'S 10S-70-3 GCMS
C6H3CI3 120-82-1 GCyS
C2H3CI3 71-55-6 GCMS
C2H3CI3 79-00-5 GCMS
C2HCI3 79-01-8 GCMS
CHCI3S 75-07-7 GCMS
CCI3F 75-69-4 GCMS
C6H3CI30 68 -OS -2 CCMS
C6H3CI30 er-9S-4 GCMS
C6H3CI30 933-75-5 CCMS
102
V
SRCH |
1
1624 8240 |
SRCH
1625 8270
SRCH
1625 8270 I
1624 8240 [
1624 8240
1624 8240
SRCH •
SRCH
1625 8270
1625 8270
SRCH [

w _.;lu


-------
\
CJ
I
f,
^*.
^
,','.
Y.
i',
1 • i'' .' " ' '. •
Toblo
I • •
Name in Regulation
2,3,4-Trichlorophsnol
•:' ! 2,4,5-Tricblorophenoxyacetic acid
ic
2,4,5-Trichlorophenoxypropionic acid
fe.
j '. 1,2,3-Trichloropropane
;••• Trichloropropane, NOS
>r i
'! -1
K •- 0,0,0-Triethylphosphorothioate
V' 3,4,5-Tr imethoxybenzaldehyde
_*'•
1
i
[-•
^;-
1,2,3-Trimethoxy benzene
sym-Tri nitrobenzene
Tr i pheny 1 ene
Tr ipropy lencglycol methyl ether
Tris(l-azridinyl)phosphine sulf ide
,'• Tris(2,3-dibromopropyl)phosphata .
!•' ..
!•''
1,3,5-Trithiano
i) Try pan blue
C: • ' .
fc'j Uracil mustard
1: : • '
A.I ITD/RCRA
Eapiricol
Foraulo
C6H3CI30
C8»5Cf303
C9H7CI303
C3H5CI3
W3PS
C10H1204
C8H1203
C6H3N306
C18H12
C10fl21°3
C6N12N3PS
C9H1504Br6P
C3H6^3
C34H24N6014S4f
C8HllCI2N302
COMPOUND DATA
CAS Nudber
15950-65-0
93-70-5
83-72-1
96-18-4
1-37-1
126-68-1
8S-81-7
634-38-6
99-35-4
217-59-4
20324-33-8
62-24-4
126-72-7
291-21-4
Js4 72-57-1
66-75-1
(Continued)

AnaJyeio RCRA
Typa Uothod Method Othar
GCMS
CCEC
GCEC
GCMS
GCMS
MS-PROB
GCMS
CCMS
HPLC
CCMS
GCMS
HPLC
MS-PROB
CCMS
HPLC
HPLC
SRCH
615 8150
615 8150
SRCH
SRCH
SRCH
SRCH
~
SRCH
SRCH
SRCH
SRCH
—
ww
                                                  103


-------
f:
 i/
Tab Io A.I   ITD/RCRA
                                                                                    DATA  (Continued)
Kama in Regulation
Ursa, l-ethyl-3-(5-nitro-2-thia/olyl)-
Vanadic acid (ammonium salt of)
Vanadium pentoxide ' ' '''
Vinyl acetate
Vinyl chloride
Warfarin (potassium salt)
Zinc
Zinc bis(dimethyldithiocarbamato)-.
Zinc cyanide '
Zinc phosphide
Zinc phosphide
Empirical
Formula
C7!I10N2OS
H4H«03V
W2
C4H602
C2H3CI
C19H16°4K
Zn
C6H12N2S4Zn
C2N2Zn
P2Zn3
P2Zn
. CAS Mumbor
B1-52-S
7603-55-6
1314-82-1
108-OS-4
75-01-4
2160-86-8
7440-66-S
137-30-4
557-21-1
*
1314-84-7
12037-79-5
Ann lysis
Typo CSathod
HPLC
ICP — •
GCMS SRCH
GCMS SRCH
GCMS 1624
—
ICP
CS2 630
ICP -- ••••
ICP
ICP
RCRA .
fJssthod Othor

6010


8240
H
6010

6C10
6010
6010
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