United States
Environmental Protection
Agency
Office of Air Quality
Planning and Standards
Research Triangle Park, NC 27711
EPA-454/R-99-044b
September 1999
Air
a EPA
Final Report - Volume II of II
Lime Manufacturing
Emissions Test Report
Chemical Lime Company
(Formerly Eastern Ridge Lime
Company)
Ripplemead, Virginia
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LIME MANUFACTURING
EMISSION TEST REPORT
CHEMICAL LIME COMPANY
(FORMERLY APG LIME COMPANY)
RIPPLEMEAD, VIRGINIA
VOLUME II OF II
APPENDICES C - F
EPA Contract No, 68D700069
Work Assignment No, 2-12
Prepared for;
Michael L. Toney (MD-14)
Work Assignment Manager
SMTG, EMC, EMAD, OAQPS
U.S. Environmental Protection Agency
Research Triangle Park, NC 27711
September 1999
p:\i532\fimpt\finalapg.rep (WP.61)
Submitted by:
PACIFIC ENVIRONMENTAL SERVICES, INC.
5001 S. Miami Blvd., Suite 300
Post Office Box 12077
Research Triangle Park, NC 27709-2077
(919) 941-0333 FAX (919) 941-0234
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DISCLAIMER
This document was prepared by Pacific Environmental Services, Inc. (PES) under EPA
Contract No. 68D70069, Work Assignment No. 2-12. The field sampling, analyses, and draft
report were completed under EPA Contract No. 68D20162, Work Assignment No. 4-01. This
document has passed PES' internal quality assurance review and has been approved for
distribution. The contents of this document do not necessarily reflect the views and policies of
the U.S. EPA. Mention of trade names does not constitute endorsement by the EPA or PES.
11
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TABLE OF CONTENTS
VOLUME I Page
1.0 INTRODUCTION 1-1
2.0 SUMMARY OF RESULTS 2-1
3.0 PROCESS DESCRIPTION 3-1
4.0 SAMPLING LOCATIONS 4-1
4.1 NO. 1 KILN 4-1
4.2 NO. 2 KILN COOLER STACK 4-1
5.0 SAMPLING AND ANALYTICAL PROCEDURES , 5-1
5.1 LOCATION OF MEASUREMENT SITES AND SAMPLE/
VELOCITY TRAVERSE POINTS 5-1
5.2 DETERMINATION OF STACK GAS VOLUMETRIC FLOW RATE ... 5-1
5.3 DETERMINATION OF DRY MOLECULAR WEIGHT AND
EMISSION CORRECTION FACTORS 5-1
5.4 DETERMINATION OF STACK GAS MOISTURE CONTENT 5-2
5.5 DETERMINATION OF POLYCHLORINATED DIBENZO-P-DIOXINS
AND POLYCHLORINATED DIBENZOFURANS 5-2
5.6 DETERMINATION OF TOTAL HYDROCARBONS 5-2
5.7 DETERMINATION OF P ARTICULATE MATTER AND METALS .... 5-6
5.8 PULVERIZED COAL WEED SAMPLING 5-6
5.9 PULVERIZED COAL FEED RATE 5-6
5.10 VISIBLE EMISSIONS 5-12
6.0 QUALITY ASSURANCE/QUALITY CONTROL PROCEDURES
AND RESULTS 6-1
6.1 CALIBRATION OF APPARATUS 6-1
6.2 ON-SITE MEASUREMENTS .' 6-4
APPENDICES A & B
VOLUME II APPENDICES C-F
111
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LIST OF FIGURES
VOLUME I
Figure 1.1 Key Personnel and Responsibility for Testing at APG Lime Company,
EPA Contract No. 68D20162, Work Assignment No. 4-01 1-2
Figure 1.2 Sampling/Monitoring Location, at APG Lime,
Ripplemead, VA 1-3
Figure 4.1 APG Lime Kiln Baghouse Inlet Sampling Location 4-2
Figure 4.2 APG Lime Kiln Baghouse Outlet Sampling Location 4-3
Figure 4.3 APG Lime Cooler Stack Sampling Location 4-4
Figure 5.1 Method 23 CDD/CDF Outlet Sampling Train 5-3
Figure 5.1 A Method 23 CDD/CDF Inlet Sampling Train 5,4
Figure 5.2 Method 25A Measurement System for THC 5-5
Figure 5.3 Method 29 Particulate Matter/Metals Baghouse Outlet and Cooler
Sampling Train 5-7
Figure 5.3A Method 29 Particulate Matter/Metals Inlet Sampling Train 5-8
Figure 5.4 Method 29 Sample Recovery Scheme (Sample Fractions 1-4) 5-9
Figure 5.5 Method 29 Sample Recovery Scheme (Sample Fraction 5) 5-10
Figure 5.6 Method 29 Sample Preparation and Analysis Scheme 5-11
IV
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LIST OF TABLES
VOLUME I
Table 2.1 Emissions Test Log APG Lime Company - Ripplemead,
VA 2-2
Table 2.2 CDD/CDF Emissions Sampling and Exhaust Gas Parameters
Kiln No. 1 Baghouse Inlet, APG Lime Company -
Ripplemead, VA 2-4
Table 2.3 CDD/CDF Exhaust Gas Concentrations and Emission Rates
Kiln No. 1 Baghouse Inlet, APG Lime Company -
Ripplemead, VA 2-5
Table 2.4 CDD/CDF Exhaust Gas Concentrations and 2378 Toxic Equivalent Stack
Gas Concentrations Adjusted to 7 Percent Oxygen, Kiln No. 1 Baghouse
Inlet, APG Lime Company - Ripplemead, VA 2-6
Table 2.5 CDD/CDF Emissions Sampling and Stack Gas Parameters
Kiln No. 1 Baghouse Outlet, APG Lime Company -
Ripplemead, VA 2-7
Table 2.6 CDD/CDF Stack Gas Concentrations and Emission Rates
Kiln No. 1 Baghouse Outlet, APG Lime Company -
Ripplemead, VA 2-8
Table 2.7 CDD/CDF Stack Gas Concentrations and 2378 Toxic Equivalent Stack
Gas Concentrations Adjusted to 7 Percent Oxygen, Kiln No. 1 Baghouse
Outlet, APG Lime Company - Ripplemead, VA 2-9
Table 2.8 Particulate/Metals Emissions Sampling and Exhaust Gas Parameters
Kiln No, 1 Baghouse Inlet, APG Lime Company - Ripplemead, VA .... 2-11
Table 2.9 Particulate Matter Concentrations and Emission Rates, Kiln No. 1
Baghouse Inlet, APG Lime Company - Ripplemead, VA 2-12
Table 2.10 Exhaust Gas Metals Concentrations and Emission Rates, Kiln
No. 1 Baghouse Met, APG Lime Company - Ripplemead, VA ......... 2-13
Table 2.11 Particulate/Metals Emissions Sampling and Stack Gas Parameters
Kiln No. 1 Baghouse Outlet, APG Lime Company - Ripplemead, VA .. 2-15
Table 2.12 Particulate Matter Concentrations and Emission Rates, Kiln No. 1
Baghouse Outlet, APG Lime Company - Ripplemead, VA 2-16
Table 2.13 Stack Gas Concentrations and Emission Rates, Kiln No. 1 Baghouse
Outlet, APG Lime Company - Ripplemead, VA 2-17
Table 2.14 Summary of Total Hydrocarbon Emissions - Kiln No. 1
APG Lime Company - Ripplemead, VA 2-18
v
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LIST OF TABLES (Concluded)
Table 2.15 Particulate/Metals Emissions Sampling and Stack Gas Parameters
Kiln No. 2 Cooler Exhaust Stack, APG Lime Company -
Ripplemead, VA 2-19
Table 2.16 Particulate Matter Concentrations and Emission Rates, Kiln No. 2
Cooler Exhaust Stack, APG Lime Company - Ripplemead, VA 2-21
Table 2,17 Stack Gas Concentrations and Emission Rates, Kiln No. 2
Cooler Exhaust Stack, APG Lime Company - Ripplemead, VA ........ 2-22
Table 5.1 Sources, Test Parameters, and Test Methods Summary
APG Lime Company - Ripplemead, Virginia 5-2
Table 6.1 Summary of Temperature Sensor Calibration Data 6-2
Table 6.2 Summary of Pitot Tube Dimensional Data 6-3
Table 6.3 Summary of Dry Gas Meter and Orifice Calibration Data 6-5
Table 6.4 Summary of Orsat Analyzer Calibration Results 6-7
Table 6.5 Summary of Method 23/Proposed Method 29 Field Sampling
QA/QC Data 6-8
Table 6.6 Summary of Calibration Gas Cylinders 6-9
Table 6.7 Summary of Method 23 Standards Recovery Efficiencies 6-10
Table 6.8 Summary of Method 29 Analysis QC Data 6-11
VI
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CASE NARRATIVE
Analysis of Samples for the Presence of
Polychlorinated Dibenzo-p-Dioxins and Dibenzofurans by
High-Resolution Chromatography / High-Resolution Mass Spectrometry
Method 23 (6/93)
Date: November 12,1996
Client ID: Pacific Environmental Services
P.O. Number: 104-97-0026
TO Project Number: 3929Ir 1
This report should only be reproduced in full. Any reproduction of this report requires permission from Triangle
Laboratories, Inc.
Rev. 06/02/95
Triangle Laboratories, Inc.
801 Capitola Drive P.O. Box 13485
Durham, NC 27713-4411 Research Triangle Park, NC 27709-3485
919-544-5729 Fax # 919-544-5491 «
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Triangle Laboratories, Inc. November 12,1996
Case Narrative 3929 Irl
Overview
Seven M23 samples, including one field blank, were received from Pacific Environmental
Services at 6°C in good condition on October 19, 1996 and were stored in a refrigerator
at 4°C. The samples and any associated QC samples were extracted and analyzed
according to procedures described in the Triangle Laboratories' Data User's Manual (Rev.
12/92-HK-2-AH-2/93). Any particular difficulties encountered during the sample handling
by Triangle Laboratories will be discussed in the QC Remarks section below. Results
reported relate only to the items tested.
Quality Control Samples
A laboratory method blank, identified as the TLI Blank, was prepared along with the
samples.
Quality Control Remarks
This release of this particular set of Pacific Environmental Services analytical data by
Triangle Laboratories was authorized by the Quality Control Chemist who has reviewed
each sample data package individually following a series of inspections/reviews. When
applicable, general deviations from acceptable QC requirements are identified below and
comments are made on the effect of these deviations upon the validity and reliability of the
results. Please consult Triangle Laboratories' Data User's Manual for further details.
Specific QC issues associated with this particular project are:
Sample Preparation Laboratory: None
Mass Spectrometry: None
Data Review: The original analyses of the samples exhibited percent recoveries that were
approximately double the expected values for all samples except the field blank sample.
Cleanup of the archived portion yielded very similar results. After consultation with
Quality Assurance, the interpretation of the results is that all of the samples, except the
field blank, were inadvertantly fortified with twice the intended amount of internal
standard (double spiked). The sample calculations are correspondingly adjusted to
account for the double internal spike, and the data are reported as such. The possible
effect on the resulting data, using the most conservative interpretive approach, is that the
reported analyte data may be artificially high by as much as two-fold. However, given the
evidence to support the double spike, this is not believed to be likely.
Other Comments: Any analytes found in the TLI Blank are detected at a level equal to or
less than the Target Detection Limit. This level of contamination is acceptable as per TLI
guidelines. OCDD is not subject to blank contamination criteria as per TLI guidelines.
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Triangle Laboratories, Inc. November 12,1996
Case Narrative 39291rl
Sample Calculations:
Analyte Concentration
The amount of any analyte is calculated using the following expression.
Ao*Qp
Amt(a)=
Ap * RRF(0) * W
Where:
Amt (0) is the amount of a given analyte,
AO is the integrated current for the characteristic ions of the analyte,
Ap is the integrated current of the characteristic ions of the corresponding internal
standard,
Qp represents the amount of internal standard added to the sample before extraction,
RRF«j) is the mean analyte relative response factor from the initial calibration (ICal) and,
W is the sample weight or volume (W = 1 for M23)
The amount is expressed in nanograms (ng) or picograms (pg).
Detection Limits
The detection limit reported for a target analyte that is not detected or presents an analyte
response that is less than 2.5 times the background level is calculated by using the
following expression. The area of the analyte is replaced by the noise level measured in a
region of the chromatogram clear of genuine GC signals multiplied by an empirically
determined factor. The detection limits represent the maximum possible concentration of
a target analyte that could be present without being detected.
2 * 2.5 * (F * H) * Qp
DL(0) =
Ap * RRF(0) * W
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Triangle Laboratories, Inc. November 12,1996
Case Narrative 3929Irl
Where:
DL(0) is the estimated detection limit for a target analyte,
2.5 is the minimum response required for a GC signal,
F is an empirical number that approximates the area to height ratio for a GC signal. This
number is 5 for the DB-5 GC column and 3.5 for the DB-22S GC column,
H is the height of the noise
Ap is the integrated current of the characteristic ions of the corresponding internal
standard,
Qp represents the amount of internal standard added to the sample before extraction,
RRF(0) is the mean analyte relative response factor from the initial calibration (ICal) and,
W is the sample weight or volume
The detection limit is expressed in nanograms (ng) or picograms (pg).
Other sample calculations may be found in the Triangle Laboratories Data User's Manual.
Data Flags
In order to assist with data interpretation, data qualifier flags are used on the final reports,
as discussed in Triangle Laboratories' Method 23 Data User's Manual. Please note that all
data qualifier flags are subjective and are applied as consistently as possible. Each flag has
been reviewed by two independent Chemists and the impact of the data qualifier flag on
the quality of the data discussed above. The most commonly used flags are:
A 'B' flag is used to indicate that an analyte has been detected in the laboratory method
blank as well as in an associated field sample. The 'B* flag will be used only when the
concentration of analyte found in the sample is less than 20 times that found in the
associated blank. This flag denotes possible contribution of background laboratory
contamination to the concentration or amount of that analyte detected in the field sample.
Under Triangle Laboratories guidelines, a laboratory blank is acceptable if the terra-
through hepta-CDD/CDF levels are all below the target detection limits (TDLS) or if the
contamination levels are less than 5% of the levels detected in the associated field samples.
If these conditions are satisfied or if the blank is unable to be reextracted, the
interpretation of the contamination levels relative to the samples should be as follows: 1)
analyte quantitations should be considered valid if the level of blank contamination is less
-------
Triangle Laboratories, Inc. November 12,1996
Case Narrative 3929 Irl
than five percent of the level detected in the field sample, 2) analyte quantitations should
be considered estimated if the analyte level in the sample is five to twenty times the level
of the analyte in the blank, or 3) analytes whose level in a sample is the same as or less
than five times the level detected in the associated blank should be considered present
likely due to laboratory contamination and not native to the sample.
An *E' flag is used to indicate that an PCDF peak has eluted at the sample time as the
associated diphenyl ether (DPE) and that the DPE peak intensity is ten percent or more of
the PCDF peak intensity. Total PCDF values are flagged 'E1 if the total DPE contribution
to the total PCDF value is greater than ten percent. All PCDF peaks that are significantly
influenced by the presence of DPE peaks are quantitated with EMPC values, regardless of
the isotopic abundance ratio. These EMPC values are most likely overestimated due to
the DPE contribution to the peak area.
An 'I' flag is used to indicate labeled standards have been interfered with on the GC
column by coeluting, interferent peaks. The interference may have caused the standard's
area to be overestimated. All quantitations relative to this standard, therefore, may be
underestimated.
A 'PR' flag is used to indicate that a GC peak is poorly resolved. This resolution problem
may be seen as two closely eluting peaks without a reasonable valley between the peak
tops, overly broad peaks, or peaks whose shapes vary greatly from a normal distribution.
The concentrations or amounts reported for such peaks are most likely overestimated.
A *Q' flag is used to indicate the presence of QC ion instabilities caused by quantitative
interferences. Affected analytes may be overestimated or underestimated as a result of this
interference. A peak is flagged *Q* only if it is affected by a QC ion deviation greater than
20% full scale as determined relative to the labeled standard against which it is
quantitated. Total PCDF/PCDF quantitations will be flagged 'Q' if the interferences affect
ten percent or more of the total PCDD/PCDF peak areas.
An *RO' flag is used to indicate that a labeled standard has an ion abundance ratio that is
outside of the acceptable QC limits, most likely due to a coeluting interference. This may
have caused the percent recovery of the standard to be overestimated. All quantitations
versus this standard, therefore, may be underestimated.
A *U' flag is used to indicate that a specific (2,3,7,8-substituted) isomer cannot be
resolved from a large, coeluting interferent GC peak. The specific isomer is reported as
not detected as a valid concentration/amount cannot be determined. The calculated
detection limit, therefore, should be considered an underestimated value.
A * V flag is used to indicate that, although the percent recovery of a labeled standard may
be below a specific QC limit, the signal-to-noise ratio of the peak is greater than ten-to-
-J
-------
Triangle Laboratories, Inc. November 12,1996
Case Narrative 3929M
one. The standard is considered reliably quantifiable. All quantisations derived from the
standard are considered valid as well.
By our interpretation, the analytical data in this project are valid based on the guidelines
of EPA Method 23 (6/93) and Triangle Laboratories' Method 23 Data User's Manual.
Any specific QC concerns or problems have been discussed in the QC Remarks section of
this case narrative with emphasis on their effect on the data. Should Pacific
Environmental Services have any questions or comments regarding this data package,
please feel free to contact our Project Scientist Selena Armistead, at (919) 544-5729, ext,
268.
For Triangle Laboratories, Inc.,
Report Preparation Quality Control
Rose West
Report Preparation Chemist Report Preparation Chemist
The total number of pages in the data package is :
-------
TRIANGLE LABORATORIES, INC.
LIST OF CERTIFICATIONS AND ACCREDITATIONS
ENVIRONMENTAL
American Association for Laboratory Accreditation. Expires July 31, 1997. Certificate
Number 0226-01, Accreditation for technical competence in Environmental Testing.(Including
Waste Water, Sol/Haz Waste, Pulp/Paper, and Air Matrices) Parameters are AOX/TOX, Volatiles,
Pesticides, PCB's, BNA's, and Dioxin/Furan. Method 1613 for Drinking Water.
State of Alabama, Department of Environmental Management Expires December 31, 1997.
Laboratory I.D. # 40950. Drinking Water for Dioxin.
State of Alaska, Department of Environmental Conservation. Expires December 31, 1996.
Drinking Water for Dioxin.
State of Arizona, Department of Health Services. Expires May 26, 1997. Certificate #AZQ423.
Drinking Water for Dioxin, Dioxin in WW and S/H Waste.
State of Arkansas, Department of Pollution Control and Ecology. Expires February 14,
1997. Primary No. 94-06497. Pulp/paper, soil, water, and Hazardous Waste for Dioxin/Furan;
AOX/TOX.
State of California, Department of Health Services. Expires August 31, 1997. Certificate
#1922. Selected Metals in Waste Water; Volatiles, Serni-volatiles, and Dioxin/furan in WW and
Soi/Haz Waste. Dioxin in Drinking Water.
State of Connecticut, Department of Health Services. Expires September 30, 1997.
Registration # PH-0117. Dioxin in Drinking Water.
Delaware Health and Social Services. Expires December 31,1996. Certificate #NC 140, Dioxin
in drinking Water.
Florida Department of Health and Rehabilitative Services. Expires June 30, 1997.Dioxin in
DW. Drinking Water ID HRS# 87424. Metals, Extractable Organics (GC/MS), Pesticides/PCB's
(GC) and Volatiles (GC/MS) in Environmental Samples. Environmental water ID HRS# E87411.
Hawaii Department of Health. Expires March 1, 1997. Dioxin in drinking water. "Accepted"
status for regulatory purposes .
Revised November 6,1996 apw Triangle Laboratories, Inc.
c «OR 801 Capitola Drive P.O. Box 13485
s, ii96 Durham, NC 2771^4411 Research Triangle Park, NC27709-3485
919-544-5729 Fax # 919^44-5491
-------
Idaho Department of Health and Welfare. Expires November 30, 1997. Dioxin in Drinking
Water.
State of Kansas, Department of Health and Environment Expires January 31, 1997.
Environmental Analyses/Nan potable Water and Solid and Hazardous Waste. Method 1613 for
drinking water. !D #'s - Drinking water and/or pollution control - E-215. Solid or Hazardous Waste -
E-1209.
Commonwealth of Kentucky, Department for Environmental Protection. Expires December
31, 1996. !D#90060. Drinking Water for Dioxin.
Maryland Department of Health and Mental Hygiene. Expires September 30, 1997.
Certification #235. Drinking water by Method 1613A.
State of Michigan, Department of Public Health. Expires March 31, 1997. Drinking water by
Method 1613.
Montana Department of Health and Environmental Services. Expires December 31, 1996.
Dioxin in Drinking Water.
State of New Jersey, Department of Environmental Protection and Energy. Extended by
state. Temporary certificate until June 30, 1997 or sooner. ID #67851. BNAs and Volatiles.
Drinking water for Dioxin.
State of New Mexico, Environment Department Expires July 31, 1997. Drinking water for
Dioxin,
New York State Department of Health. Expires March 31, 1997. ID #11026. Environmental
Analyses of non-potable Water, Solid and Hazardous Waste. Method 1613 in DW.
State of North Carolina, Department of Environment Health and Natural Resources Expires
December 31,1996. Certificate # 37751. Drinking Water for Dioxin.
State of North Carolina, Department of Environment, Health, and Natural Resources,
Division of Environmental Management Expires December 31, 1997. Certificate # 485.
Metals, pesticides, semi-volatiles and volatiles; TCLP.
State of North Carolina, Department of Environment, Health, and Natural Resources -
Division of Radiation Protection. Expires april 30, 1998. General License No. 32-0875-OG;
Specific License No. 0954-1.
Revised November 6,1996 apw
Printed Novembers, 1996
-------
North Dakota State Department of Health and Consolidated Laboratories. Expires
December 31, 1996. Certificate # R-076, Effective October 4,1993. Dioxin in Drinking Water.
Oklahoma Department of Environmental Quality. Expires May 31, 1997. Laboratory #9612,
Dioxin by 1613A, 8290 and 8280.
State of South Carolina, Department of Health and Environmental Control. Expires Apnl 1,
1997. Certificate number #99040001 (drinking water). Expires August 31, 1997. Certificate
number #99040002 (other parameters). Dioxin/Furans, BNA, Volatiles, and PCBs/pesticides
under Clean Water Act, 2,3,7,8-TCDD for Drinking Water, and Organic extractables for Solid and
Hazardous Waste.
State of Tennessee. Department of Environment and Conservation. Expires February 5,
1999. ID #02992. Method 1613 Drinking water only.
U.S. Department of Agriculture Soil Permit Expires September 30, 2001. Permit No. S-3790
Revised. Under the authority of the Federal Plant Pest Act, permission is granted to receive
foreign soil samples for use in labatory analysis.
U.S. Army Corps of Engineers. Expires November 30, 1997. Validated to perform methods
8280 & 8290 for Lockboume Landfill Site Investigation, Defense Distribution Depot Projects, and
assorted projects for the USAGE North Pacific Division Laboratory.
U.S. EPA Region V. Expires December 29, 1995. Dioxin in Drinking Water.
U.S. EPA Region VIII, for the State of Wyoming. Expires December 31, 1996. Dioxin in
Drinking Water.
State of Utah, Department of Health. Expires December 31, 1997. Certificate Number E-166.
Certification for the following parameters: Semi-Volatiles and Volatiles under RCRA; Volatiies
under Clean Water Act; Dioxin/furans by Method 8280; Drinking water for Dioxin by Method 1613;
Metals including Mercury and Microwave Digestion.
Commonwealth of Virginia, Department of General Services, Division of Consolidated
Laboratory Services. Expires June 30,1997. ID # 00341. Dioxin in Drinking Water.
State of Washington, Department of Ecology. Expires September 11, 1997. Lab Accreditation
Number C067. Scope of Accreditation applies to water analyses for Polychlorinated Dibenzo-p-
dioxins and Polychlorinated Dibenzofurans, BNA Extr (Semivolatile) Organics and Purgeable
(Volatile) Organics.
State of Washington, Department of Health. Expires April 30, 1997. Drinking water for Dioxin.
Revised Novembers, 1996 apw
Printed November 6,1996
-------
State of West Virginia, Department of Health. Expires December 31, 1996. Certificate No.
9923(C). Drinking water for Dioxin.
State of Wisconsin, Department of Natural Resources. Expires June 30, 1997, Laboratory ID
Number 999869530. Certification for the following categories of Organics: Purgeable,
Base/Neutral, Acid, PCBs, and Dioxin,
PHARMACEUTICAL
Drug Enforcement Agency (DEA). Expires November 30, 1997. Registration number
RT01195835. Controlled substance registration for schedules 1,2,3,3N,4,5.
N.C. Department of Human Resources. Expires October 31, 1996. Registration number NC-
PT 0000 0031. North Carolina controlled substances registration. Application submitted for
renewal.
Food & Drug Administration (FDA) Registration. Expires July 1997. ID #s 001500 1053481.
Annual registration of drug establishment. Annual registration of drug establishment.
OTHER
Clinical Laboratory Improvement Amendments (CLIA) Registration. Expires May 30, 1997.
ID # 34D0705123. Department of Health & Human Services, Health Care Financing
Administration.
U.S. EPA Large Quantity Hazardous Waste Generator. No expiration date. EPA ID
#NCD982156879. Permit indicates that the laboratory is a large generator of hazardous waste.
North Carolina Radioactive Materials License. Expires April 30 1998. License No. 032-0954-
1. License authorizes the licensee to receive, acquire, own, possess, transfer, import and use
such radioactive materials as designated.
North Carolina Genera! License for Radiation Protection. No. expiration date. License No.
032-875-OG. The general license applies only to radioactive material contained in devices which
have been manufactured and labeled in accordance with specific requirements.
Revised November 6,1996 apw
Printed Novembers, 1996
10
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DOCUMENT
CONTROL
Triangle Laboratories, Inc.
801 Capitola Drive P.O. Box 13485
Durham, NC 27713-4411 Research Triangle Park, NC 27709-3485
919-544-5729 Fax # 919-544-5491
I 1
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ANALYTICAL REQUEST AND CHAIN OF CUSTODY
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-------
PAGE 2 Of 2 •
; Sook :
: MI ;
; CustooY Seal ; Present/Intact - Saiole Seals: Present ! Til Project Huiber ! 392*5]
,' Chain of Custoav : Present . Accent.Cone1.: TES t •<- ? -
! Saisle Tsas : Present ': ! Client; PESOS ! Pacific Envircniental Services
i Saioie lag Huioers: listea * - ; • '
! S.10 Foras : N/A - : Date Received ! 10/19/96 IJy
; lea Chest • ICE PACKS Teio 6.0 C : Carrier and Nuabsr ! ftlXE 3
t • -"» t • 1-- —t 1 --t *-- »—.
! TU ,'luaoer natrix ! To LA3 ! To STORAGE! To U8 ,' To STORAGE! To IA3 ! To STORAGE! To ARCHIVE,' DISPOSED !
! nR/H:C?fi Client 10 location! Oate/Init ! Data/Init ! Oate/Init ! Oate/Init ! Dats/Inil 1 Date/lint ! Oate/Init ! Date/Init :
t + t f.~~~~* + *" + f *•
! 143-23-58
238-2
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! Recaivina Reiarks:
! Archive fle»arxs:
LABORATORIES. INC.-LOG IN RECORD/CHAIN Of CUSTODY-REVISED 06/13/1996-
-------
TRIANGLE LABORATORIES, INC.
SAMPLE TRACKING AND PROJECT MANAGEMENT FORM
TLI Proj#: 39291-rl
Prod Code: D23061
DetectLim: .05 ng
-ADMINISTRATIVE INFORMATION -
Samples: 7
Matrix.: M23Train
Type...: A
Recvd..: 10/19/96
TurnAround.
Hold Time..
Start Date.
Date Due,..
DWL Due Dt.
21 Day(s)
14 Day(s)
10/19/96
11/09/96
10/29/96
Analyte List.: Tetra-Octa PCDDs/PCDFs
Method.......: Method 23:Tetra-Octa (Tol Combined)
Client Proj..; Eastern Ridge Lime Facility
Client.......: Pacific Environmental Services (PESOS)
P.O. No : 104-97-0026 Collect Dt/Tm: 10/16/96
Contact : Frank Meadows Phone : 919-941-0333
Proj . Mgr. . . . : Selena Armistead Fax : 919-941-0234
Sample Origin:
SPECIAL INSTRUCTIONS / QA REQUIREMENTS
Prep Project: 03117 Prespike Standard: USD-C, USD-S
TEF : EPA ' 89 Prespike Amount. . : 4, Ong
Extraction Exp...: 10/30/96
REPORTING REQUIREMENTS-
Reporting Format: Report Option II
See MILES for Instructions/Communications.
Completed by:
Reviewed by:
DATE;
DATE:
J-Sfc/91
(PMGT0395)
•» C
I b
-------
PESOa-Pacific Environmental Services
238~2
1=1 '""O J eo-fc ; 39291
143—23 —SB
PESOS-Pacific Environmental Services
238-2
Rr-oJ
-------
PES03-Pac1fic Environmental Services
23A— 1
ct = 3 9 2 9 -,
1 -4-3—23 — 1 B
PES03-Paclfic Environmental Services
23A~ 1
ot : 39291
— 23— 1 A
PES03-Pac1flc Environmental Servfcts
23A-2
Project;39291
1 -4-3— 23— 2B
PE^§oarPsfc1f1c Environmental Services
i V, 2 3 A-2
PfO J oct;39291
I*,-* 3 — 2 3 — 2 A
PES03-Pac1fic Environmental Service.
23A-3
23—3B
PES03-Pac1f1c Environmental Services"
23A-3
Pr-oJ^c-t; 39291
143—23—30
t n
PES03
-Pac1f1c Environmental Services
PES03-Pac1f1c Environmental Services
DATE W/11/96 TLZ BLANK
SPIKE 4.0ng USF-C & USF-S
SPIKEK £3^5
PREPARES "G.L.
PICIFIC ENVIRONMENT
j
J
(^
-S03-Pac1fic Environmental Services
Project : 3
1 ,4.3— 23 —
t : 39291
-------
Date: 10/21/96
Time: 22:15
Sample
ft crd TLI_Number.. Customer.Sample.Id
000 TL1 Blank TLI M32 Blank
001 143-23~1A,B 23A-1
002 143-23-2A.B 23A-2
003 143-23-3A-C 23A-3
004 143-23-4A.B 23B-1
005 143-23-5A.B 23B-2
OOS 143-23-6A-C 23B-3
007 143-23-7A.B 23FB-4
TRIANGLE LABORATORIES, INC.
Met Lnb MM5/PUF Ohsrrvot ions
Prrv|i-t!|-! 31291.
F. XAD Filter Glass Wool PUP
No Color Color Color Color .
WHITE NO WHITE NA
1 WHITE GRAY WHITE NA
1 WHITE GRAY WHITE NA
1 WHITE LT GRAY WHITE NA
3 WHITE GRAY WHITE NA
1 WHITE GRAY WHITE NA
2 WHITE LT GRAY WHITE NA
1 WHITE WHITE WHITE NA
Air
. . Odor. . . . Q.No. Entered. By. ,
NO 03II7 ADKINS
NO 03117 ADKINS
NO 03117 A0KIHS
HO 03117 ADKINS
NO 03117 ADKINS
NO 03117 ADKINS
NO 03117 ADKINS
NO 03117 ADKINS
- . Date,
10/21
10/21
10/21
10/21
10/21
10/21
10/21
10/21
22;
22:
22:
22:
PRDPERC V3.19
Page : 1
Time S
14 F
14
14
14
22:14
22:
22s
22:
14
14
14
F
P
F
F
F
P
F
r
*** End of Regort ***
-------
| TRIANGLE LABORATORIES, INC. PAGE 1 0? 1 [
| Oioxin Sample Preparation Tracking 6 Management Form |
| Project: 39291 Client: ?acific Environmental Services (PESOS! |
| Solvent (sj /Acid (s! : foU*^*'"'1 ***/ / Method: Mechod 23:T«era-Oer_a (Tol (Vmhmvrl)
| Lot Numbers: *J ft 2. fj 2- / / Extraction Date: f (j / ? ,? / T 4y
j IS Spite: 40 pi cone: 0.1000 ng/pl
j SS Siaike- MQ ^l cone- £ t^D^ ng/pl « « ">-T ' •*•--
| MS Soike: 0 ul cone: 0.0000 nq/wl | "XT f \ ' /LP/K1 I 1
1 LCS Soike: 0 pi cone: 0.0000 rug/ pi ^.M rf, 1 ¥2^?^ 3>T*714 A-| | I
1 OPR Soike: -M-;i,l i.U'nlT 9-re* — ng/>it->. UjMJfi [Ulr-J'li''?»'A I i
I | Til / i GROSS I SAMPLE | 10, / 2-/ /% | /_£_ /^ /j£\ _/_/_!_
|S».crd| SAMPLE / CLIENT I WEIGHT | SIZE | p-^ngAil I C, i ng/jil 1 ng/nl 1
| . | ID / SAMPLE ID 1 Before After | g / ml | V* ® <*1 *«3 111 1 Ml 1
i i TLI Blank 1 | | | - | /|, | j
(000 | TLI M32 Blank ] | | I \ L. * T~\- * C-T"/ \ 1
i | 143-23-1A.B 1 | | , 1 A I /rL* 1 1
|001 | 23A-1 | | | / • /H | ^l/ ! |
1 | 143-23-2A.B | | | A \ /U |
|002 | 23A-2 | i if /__ • /-I | (My I I
| i 143-23-3A-C | | | i , /( I X^ ] I
|003 | 23A-3 | | |t 1 L-n. '(W' \ \
1 ! 143-23-4A.B | 1 1 I i /1\ i 1
]004 j 23B-1 | | | ' | £_ _^ 1 i/^ | |
1 | 143-23-SA.B | | 1 i . A | /Jlv | |
1005 | 23B-2 | ] | 1 | L- -A,, 1 ^f | |
,. . + + + + + "..^ + + __
| | 143-23-6A-C 1 | ,| / A l /)fi/ l l
|OOS | 23B-3 | | ! 1 i L . A. 1 \C¥ I I
*-. ...... ....* ...* 4- * + - 1-* V.J. 4.-,,,.. _,.»_.+ _-
* * «.*-.--+ -- +.«. -* -».+ «. * * ^ ^.
i | 143-23-7A.B i ] | / A ' /*1^ ' '
|007 I 23FB-4 | | | 1 | L • H, I F|/ 1 1
II 111 111
II ! i 1 i 1
II 1 I 1 1 1 i 1
II 1 ! 1 ! 1 1 I
| Gross weight of sample container *• sample before/after aliquot removal,
i 1 f i/^i 1 ^ J^ ~t:i /\ ^T 11 § i » C S» fi L 1 i Wtfm ?\ *9t fan- / f*£ t
1 Conotsfltnts j f o ^*i ^wr' / LL fli ^w- ^ - ^J *^ if / w« A c_ %_,/ <*T ' ij\ ^" t— i i V I 1 ™\ *•* ' ^* *
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Matrix- lU 1 3
I
1 Chemist |
iSoike # j
| " ID |
_/_/_! " Expiri
/ / I " Date |<
ng/Ml 1 " Cone . I
Ml ! "Vol.
|Any Left
! yes /no
JAny f.eft
j yes /no
1 yes/no |
(Any Le£t §
s
I yes/no
iAny Left
| yes/no
] Any Left
| yes/no |
|Any Left|
| yes /no
[Any Left
| yea /no ',•
|Any Left]
'• ye 'i ITUJ j
(Any Left)
| yes/no |
1
i
i i
! 1
! fetfMirV •y?^^ initials: X_C_
Date:(jL/H./^S 1
- I
XXXXX . Gross Weight not provided for HATER Samples. I
REV 09/12/96 (PSTMF 7)-- +
| Initials of both SPIKER AHD OBSERVER must be entered.
-------
PAGE 1 OF 1
TRIANGLE LABORATORIES, INC.
DIOXXH SAMPLE EXTRACTION and CLEANUP TRACKING FORM
TLI Project Ho.; 39291
Ext Sft.crd and | /, |/ ^ 1 I -T\, 1 /V?\ I/ /^N ' A? 1 ' ( C^ ' ( 9 ) ' ' '
TLI Number U_^' V^L) i ^_J ( T )( 6 ) l( / / W 1 W % 1
j ^**-™^^ ^^ ^ \^ _X^ X ^ ^^^ _ 1
000 ' k^ i 4pv^/i^^' i i /IL t^*' i I'tl'- u'/V^v"'^
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004 /' |
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143-23-SA-C | i | |
007 U> | .
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Enter the procedure number below into the
Initial and date each sample for each nun
# . . . . .. . ... . . . PROCEDURE DETAILS
7 ) '"tiPTKiP>M"i.'KH EXTRACT-TOW
3-^*^ADD TKxDECA»E
* X'SfflT.QVSiP 4 OmL /
5} COMBINE
6) jjVJDJCg I.IPID DSTERMIHATIOII ^D.*5^
8)
-------
PAGE 1 OF 1
TRIANGLE LABORATORIES, INC.
DIOXIN SAMPLE EXTRACTION and CLEANUP "TRACKING FORM
TLI Project No.: 39291 rl
Ext St.crd and
TLI Number 1 ~7 1 v^
TLI B°L !wf)^ ^
rl ooi | '^r^P^I
143-23-lA,B LpTr 1 ^V
"+ "*" ,
rl 002 III
143-23-2A.B | 1 |
rl 003 | 1 |
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1 1 1
i 11 1
1 1 i 1 1
II 1 1 1 1
Enter the procedure number below into the box at the top of each column to signify the step performed. |
Initial and date each sample for each numbered procedure performed. ' "|
I
# PROCEDURE. DETAILS (circle) |
1) EXTRACTION ON_ OFF Soxhlet / Jar / Sep Funnel / Steam Dlst / Cent LL / ASE / Waste Dilution |
2! SPIKE AFTER EXTRACTION |
3) MJD TRIDECANE j
4) ROTOVAP 40wL / lOmL / Dryness |
S) COKBINS |
6) DIVIDE / LIPID DETERMINATION |
7) SOLVENT EXCHANGE [
8) CLEANUP (gSP~26q) / DSP 240 /. DSP 225 / DSP 215 / E010401 / Other |
9) TRANSFER |
10) ADDITIONAL CLEANUP DSP 260 / DSP 240 / DSP 225 / DSP 215 / 1010401 / Other |
11) FINAL TRANSFER I
Comments:
=Rev 09/12/96 (PSTMF 4)==+
92
-------
PAGE 1 OF 1
TRIANGLE LABORATORIES, INC.
Transfer Chain-of-Custody Form
Project 39291-rl
Transfer From: DWLH5 To: DMS5
Initials. . Date Time
Released by: j^fOf) /Q /^] fff}
;„. i *.
Accepted by:
MILES.ID,
39291-rl
39291-rl
39291-rl
39291-rl
39291-rl
39291-rl
39291-rl
39291-rl
TLI No,
Cust.Id,
-000
-001
-002
-003
-004
-005
-006
-007
TLI
143
143
143
143
143
143
143
Blank
-23-lA,B
-23-2A,B
-23-3A-C
-23-4A,B
-23-5A,B
-23-6A-C
-23-7A,B
TLI M32 Blank
23A-1
23A-2
23A-3
23B-1
23B-2
23B-3
23FB-4
Additional comments or instructions:
-XfrCOC (Rev 11/01/94}--+
-------
PAGE 1 OF 1
| TRIANGLE LABORATORIES, INC.
| Method: Method 23:Tetra-Octa (Tol Combined! HR GC/HSMS ANALYSIS
Required Detection Limit : . OS ng
1
| 1ST COLDMH
| | TLI / | • GC/MS FILENAME |
|S#.crd| SAMPLE ID / CLIENT | COLDMN; V).fl J |
| j / SAMPLE ID | 1
|rl TLI Blank _J jp"\ (. Ouia &Q
i °°° 1 T« M32 Wank' jl^ k QS £^J
|rl | 143-23-1A.B | ^'fa&CfO 1 |
001 | 23A-1 [
|rl | 143-23-2A.B | '' llCt CjG f2— \
|002 | 23A-2 |
1
| PROJECT; 392Slrl |
SAMPM INFORMATION RS Cono |
2ND COLDMN 20 Ml a 0.1 NG/jil |
CONFIRM | CONFIRM FILENAME |USF-RS
ICOLOMN; T) Ql*~{ IVOLOME
| ISOLN i
1 1
^LyO |
Xp23-j i
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|007 23FB-4 |
1 1
1 1
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1 1
1 1 1
1 1 1
1 1 I
1 1
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Type:. A
Spike File: SPX23704
Ame of Extracts 50%
91
-------
I'BIMfiliE
TH£
RUN LOG
MS*
7«r
COLUMN WE
tyar CUD^
COLUMN tt
GIG^US
HOI NAME
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AMOUHI INJ
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c/c
£ Pcuf
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IIME
PROJECT*
SAMPLE*
No
CLIENT SAMPLE 10
cowEHrs
332;
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IPAGE
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-------
TH£
RUN LOG
C\J
HS«
^5T
COLUHN TYPE
P65 66m oz^
COLUMN U
(p/tol^P>
PI OT HAKE
^rcA^o
PKD
"7Zx2-
AMQUHI 1HJ
Q^W
ACQUISITION
£P^u
-------
TRIflNGr.E TABORATORTES TMC
RUN LOG
CM
HS«
>>r
COLUHH ITPE
\>^>T &CW-,
COLUMN #
GvW^W
PIOI HAME
VMO
PKt>
~~^
s
AMOUNT IHJ
V,o^Jv_
ACQUISITION
E p LA/S* i.
c/c
Ft, P CuS
-------
•I'RTANGT.E TABQBATQBTE3
RUN LOG
I -
cv
HSi
v<£-.y
COLUHH TYPE
Pp-225
COLUHN #
£(£#"2-1 *>
PLOT NAME
gVTU fKD -
PICO
>
AMOUNT 1NJ
C-.VA.J
ACOUISISriON
X -
DATE
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Ho
3
CLIENT SAMPLE ID
COHHENTS
332;
OP IHII
flLE #
i
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23
61
11: (JO
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21
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PAGE
3
-------
TABORATQRIE3 TNC
RUN LOG
CM
MS*
Vc-X
COLUHH TYPE
ffa**
COLUHH #
£/ £(*\9
PLOF NAME
a/v^fKP-
PKD
_— ^?
AMOUNT IHJ
3,0 ni.
ACOUISISTIOH
vx - , *. iT" *T~T"
^CcJ#j" „ | |-
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11 ^
DATE
!IM£
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SAMPLED
Ho
CLIENT SAMPLE ID
COHHEHTS
A"3
332;
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If
PAGE
*
4
-------
SAMPLE
DATA
Triangle Laboratories, Inc.
801 Capitola Drive P.O. Box 13485
Durham, NC 27713-4411 Research Triangle Park, NC 27709-3485
919-544-5729 Fax #919-544-5491 0 n
-------
TRIANGLE LABORATORIES, INC.
Sample Result Summary for Project 39291rl
Method 23X Full Screen Analyses (DB-5)
Data File
Sample ID
Units
Analytes
2378-TCDD
12378-PeCDD
12347 8-HxCDD
123678-HxCDD
123789-HxCDD
1234678-HpCDD
OCDD
2378-TCDF
12378-PeCDF
23478-PeCDF
123478-HxCDF
123678-HxCDF
234678-HxCDF
123789-HxCDF
1234678-HpCDF
1234789-HpCDF
OCDF
TOTAL TCDD
TOTAL PeCDD
TOTAL HxCDD
TOTAL HpCDD
TOTAL TCDF
TOTAL PeCDF
TOTAL HxCDF
TOTAL HpCDF
Other Standards
37C1-TCDD
13C12-PeCDF 234
13C12-HXCDF 478
13 C 12 -HxCDD 478
13C12-HpCDF 789
Other Standards
13C12 -HxCDF 789
13C12-HxCDF 234
T966616
TLI M23 Blank
ng
(0
(0
{0
(0
<0
(0
(0
(0
(0
(0
-------
TRIANGLE LABORATORIES, INC.
Sample Result Summary for Project 39291rl
Method 23X Full Screen Analyses (DB-5)
Page 2
11/12/96
Data File
Sample ID
Units
T966604
23B-1
ng
T966605
23B-2
ng
T966612
23B-3
ng
T966607
23FB-4
ng
Analytes
2378-TCDD
12378-PeCDD
123478-HxCDD
123678-HxCDD
123789-HxCDD
1234678-HpCDD
OCDD
2378-TCDF
12378-PeCDF
23478-PeCDF
123478-HxCDF
123678-HxCDF
234678-HxCDF
123789-HxCDF
1234678-HpCDF
1234789-HpCDF
OCDF
TOTAL TCDD
TOTAL PeCDD
TOTAL HxCDD
TOTAL HpCDD
TOTAL TCDF
TOTAL PeCDF
TOTAL HxCDF
TOTAL HpCDF
(0.01)
(0.02)
(0.02)
(0.02)
(0.02)
0.05
0.34
0.16
0.02
0.03
0.04
0.02
0.02
(0.02)
0.07
0.01
0.06
0.20
0.08
0.20
0.09
1.4
0.43
0.16
0.08
B
(0.01)
(0.02)
(0.02)
(0,02)
(0.02)
0,03
{0.09}
0.07
(0.01)
(0.01)
0.02
0.006
(0.01)
(0.02)
{0.02}
(0.02)
{0.02}
0.27
0.09
0.12
0.05
0.37
0.06
0.06
{0.02}
Other Standards Percent Recovery Summary (% Rec)
37C1-TCDD 112 107
13C12-PeCDF 234 110 101
13C12-HxCDF 478 121 119
13C12-HXCDD 478 110 110
13C12-HpCDF 789 110 106
Other Standards Percent Recovery Summary (% Rec)
13C12-HXCDF 789 100 93.9
13C12-HxCDF 234 95.9 91.6
Internal Standards Percent Recovery Summary (% Rec)
(0.01)
{0.008}
(0.03)
(0.02)
(0.02)
0.04
{0.34}
0.14
(0.01)
(0.01)
0.03
0.008
{0.01}
(0.02)
0.03
(0.03)
0.06
0.61
0.12
0.13
0.04
1.2
0.26
0.05
0.03
133
123
139
124
128
104
94.4
B
(0.005)
(0.008)
(0.01)
(0.01)
(0.009)
0.01
0.18
(0.005)
(0.005)
(0.005)
(0.007)
(0.006)
0.006 B
(0.008)
0.006
(0.01)
0.02
(0.005)
(0.008)
(0.01)
0.01
(0.005)
(0.005)
0.006
0.006
96.3
93.0
103
97.3
95.8
104
93.5
13C12-2378-TCDF
13C12-2378-TCDD
13C12-PeCDF 123
13C12-PeCDD 123
13C12-HxCDF 678
13C12-HxCDD 678
13C12 -HpCDF 678
13C12-HpCDD 678
13C12-OCDD
73
76
72
66
74
83
81
84
69
.0
.8
.4
.1
.0
.0
.6
.3
.1
76
78
74
68
78
86
82
82
58
.5
.0
.4
.8
.9
.1
.1
.0
.8
64
63
56
56
72
70
• 67
71
51
.6
.0
.5
.6
.0
.6
.0
.2
.1
81
86
77
72
95
99
96
94
71
.2
.5
.7
.2
.1
.5
.3
.8
.4
{Estimated Maximum Possible Concentration}, (Detection Limit)
Triangle Laboratories, Inc.® Analytical Services Division
801 Capitals Drive • Durham, North Carolina 27713
Phone: (919) 544-5729 • Fax: (919) 544-5491
Printed; 11:51 11/12/96
31
-------
Data File
Sample ID
TRIANGLE IABORATORIES , INC.
Sample Result Summary for Project 39291rl
Method 23X (DB-225)
X964233 X964234 X964235
23A-1 23A-2 23A-3
Page 1
11/11/96
X964236
23B-1
Units ng ng ng ng
Analytes
2378-TCDF 0.03 0.02 0.03 0.04
Internal Standards Percent Recovery Summary (% Rec)
13C12-2378-TCDF 93.0 75.1 86.0 82.4
Triangle Laboratories, Inc.® Analytical Services Division
801 Capitals Drive • Durham, North Carolina 27713 Printed: 16:16 11/11/96
Phone: (919) 544-5729 * Fax: (919) 544-5491 3 2
-------
TRIANGLE LABORATORIES, INC. Page 2
' " Sample Result Summary for Project 39291rl 11/11/96
Method 23X (DB-22B)
Data File X964237 X964238
Sample ID 23B-2 23B-3
Units ng ng
Analytes
2378-TCDF 0.02 0.04
Internal Standards Percent Recovery Summary (% Rec)
13C12-2378-TCDF 82.3 71.1
Triangle Laboratories, Inc.® Analytical Services Division
801 Capitals Drive • Durham, North Carolina 27713 Printed: 16:16 11/11/96
Phone: (919) 544-5729 • Fax: (919) 544-5491 3
-------
TLI Project:
Client Sample:
39291rl
TLI M23 Blank
Method 23 PCDD/PCDF Analysis (a)
Analysis File: T966616
Client Project:
Sample Matrix:
TLI ID:
Sample Size:
Dry Weight:
GC Column:
Eastern Ridge Lime Facility
XAD Date Received: / /
TLI Blank Date Extracted: 10/21/96
Date Analyzed: 11/01/96
1.000 Dilution Factor: n/a
n/a Blank File: T966616
DB-5 Analyst: WK
Spike File:
ICal:
ConCal:
% Moisture:
% Lipid:
% Solids:
SPX23708
TF53286
T966614
n/a
n/a
n/a
2,3,7,8-TCDD
1,2,3,7,8-PeCDD
1,2,3,4,7,8-HxCDD
1,2,3,6,7,8-HxCDD
1,2,3,7,8,9-HxCDD
1,2,3,4,6,7,8-HpCDD
1,2,3,4,6,7,8,9-OCDD
2,3,7,8-TCDF
1,2,3,7,8-PeCDF
2,3,4,7,8-PeCDF
1,2,3,4,7,8-HxCDF
1,2,3,6,7,8-HxCDF
2,3,4,6,7,8-HxCDF
1,2,3,7,8,9-HxCDF
1,2,3,4,6,7,8-HpCDF
1,2,3,4,7,8,9-HpCDF
1,2,3,4,6,7,8,9-OGDF
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
0.01
ND
ND
ND
ND
0.005
0.01
0.01
0.01
0.01
0.02
0.03
0.005
0.006
0.006
0.008
0.007
1.39 25:58
0.01
0.009 .
0.01
0.03
Total TCDD
Total PeCDD
Total HxCDD
Total HpCDD
Total TCDF
Total PeCDF
Total HxCDF
Total HpCDF
0.009
ND
ND
ND
ND
ND
0.01
ND
0.01
0.01
0.02
0.005
0.006
0.01
Page 1 of 2
X237JPSR V1.M.LARS6.08.00
Triangle Laboratories, Inc.®
801 Capitola Drive » Durham, North Carolina 27713
Phone: (919) 544-5729 • Fax: (919) 544-5491
Printed: 11:50 11/12/96
-------
TLI Project: 39291rl
Client Sample: TLI M23 Blank
Method 23 PCDD/PCDF Analysis (a)
Analysis File: T966616
intemaf Standards
13C12-2,3,7,8-TCDF
»C12-2,3,7,8-TCDD
l3C,2-l,2,3,7,8-PeCDF
13Ci2-l,2,3,7,8-PeCDD
13C,2-l,2,3,6,7,8-HxCDF
13C,2-l,2,3,6,7,8-HxCDD
13C,2-l,2,3,4,6,7,8-HpCDF
13C12-l,2,3,4,6,7,8-HpCDD
13C12-1,2,3,4,6,7,8,9-OCDD
37Cl4-2,3,7,8-TGDD
13C12-2,3,4,7,8-PeCDF
I3Ci2-l,2,3,4,7,8-HxCDF
13C,2-l,2,3,4,7,8-HxCDD
13C12-l,2,3,4,7>8,9-HpCDF
Amt (ng)
6.5
6.3
5.4
5.1
6.6
6.9
5.8
6,0
7.9
%f30££Vi
81.3
78.2
66.9
63.8
82.5
86.8
72.1
75.3
49.6
4.4
4,1
4.7
4.2
2.8
111
103
117
104
68.9
Alternate Standards (Type A) Amt. (ng) %Recov<
13Ci2-l,2,3,7,8,9-HxCDF
13C,2-2,3,4,6,7,8-HxeDF
l3Ci2-l,2,3,4-TCDD
13C12-l,2,3,7(8,9-HxCDD
3.3
4,0
82.1
99.3
H-y QCLantts
40%-130%
40%-130%
40%-130%
40%-130%
40%-130%
40%-130%
25%-130%
25%-130%
25%-130%
ii|plsiiilllSlii|lliiili™
mmsm^mrnm^smm
70%-140%
70%-140%
70%-140%
70%-140%
70%-140%
ary QC Limits
40%- 130%
40%-130%
Ratio
0.74
0.79
1.45
1.52
0.49
1.21
0.41
1.03
0.88
1.46
0.50
1.19
0.41
Ratio
0.50
0.50
0.81
1.20
iff Ftags
15:37
16:25
20:53
22:20
25:21
26:11
28:19
29:16
31:43
16:25
21:52
25:15
26:06
29:36 V
IT Flags
26:41
25:56
16:10
26:30
Data Reviewer
11/12/96
Page 2 of 2
vl,14, LtBS 6.08.00
Triangle Laboratories, Inc.®
801 Capitola Drive • Durham, North Carolina 27713
Phone: (919) 544-5729 • Fax: (919) 544-5491
Printed: 11:5011/12/96 _
3 J
-------
TLI Project: 39291rl
Client Sample: TLIM23 Blank
Toxicity Equivalents Report
Analysis File: T966616
Client Project:
Sample Matrix:
TLI ID:
Sample Size:
Dry Weight:
GC Column:
Eastern Ridge Lime Facility
XAD Date Received: / /
TLI Blank Date Extracted: 10/21/96
Date Analyzed: 11/01/96
1.000 Dilution Factor: n/a
n/a Blank File: T966616
DB-5 Analyst: WK
Spike File:
ICal:
ConCal:
% Moisture:
% Lipid:
% Solids:
SPX23708
TF53286
T966614
n/a
n/a
n/a
Analyses
2,3,7,8-TCDD
1,2,3,7,8-PeCDD
1,2,3,4,7,8-HxCDD
1,2,3,6,7,8-HxCDD
1,2,3,7,8,9-HxCDD
1,2,3,4,6,7,8-HpCDD
1,2,3,4,6,7,8,9-OCDD
TOTAL PCDD
2,3,7,8-TCDF
1,2,3,7,8-PeCDF
2,3,4,7,8-PeCDF
1,2,3,4,7,8-HxCDF
1,2,3,6,7,8-HxCDF
2,3,4,6,7,8-HxCDF
1,2,3,7,8,9-HxCDF
1,2,3,4,6,7,8-HpCDF
1,2,3,4,7,8,9-HpCDF
1,2,3,4,6,7,8,9-OCDF
TOTAL PCDF
Amt.{ng)
0.005
0.01
0.01
0.01
0.01
0.02
0.03
0.005
0.006
0.006
0.008
0.007
0.01
0.01
0.009
0.01
0.03
Total
X
X
X
X
X
X
X
X
X
X
X
X
X
X
x
X
X
EPA TEFs,
18F
l =
0.5
0.1
0.1
0.1
0.01
0.001
0.1
0.05
0.5
0.1
0.1
0.1
0.1
0.01
0.01
0.001
1989a: 0.0208 ng
EquiVafent
0.005
0.005
0.001
0.001
0.001
0.0002
0.00003
0.0132
0.0005
0.0003
0.003
0.0008
0.0007
0.001
0.001
0.00009
0.0001
0.00003
0.00752
Page 1 of 1
TEFPR v
, LARS S.«jOO
Triangle Laboratories, Inc.®
801 Capitals Drive * Durham, North Carolina 27713
Phone: (919) 544-5729 • Fax: (919) 544-5491
Printed: 11:51 11/12/96
3
I)
-------
Data Review By:
Initial ---- Date...
KM\fJ I ' /If
Calculated Noise Area:
2.62
The Total Area for each peak with an ion abundance ratio outside
ratio limits has been recalculated according to method requirements.
Page No.
11/11/96
Listing of T966616B.db£
Matched GC Peaks / Ratio / Ret. Time
Compound/
M_Z,... QC.Log Omit Why ..RT. OK Ratio Total.Area... Area.Peak.1.. Area.Peak.2.. Rel.RT Compound.Name.. ID.
TCDF
304-306
304-306
13C12-TCDF
316-318
316-318
TCDD
320-322
320-322
37C1-TCDD
328
328
DC
DC
DC
DC
DC
DC
DC
DC
DC
DC
DC
DC
DC
DC
DC
DC
DC
DC
DC
DC
DC
DC
NL
SN
SN
SN
SN
0
NL
WH
4
NL
SN
SN
SN
SN
SN
SN
SN
SN
SN
SN
SN
SN
WH
WH
1
Os 00
12:59
13:27
14:47
15:39
Peaks
0:00
14:40
15:12
15:37
16:05
17:37
Peaks
0:00
14:57
15:26
15:37
15:46
15:56
16:10
16:25
16:36
17:04
17:11
17:17
17:45
17:49
17:53
17:59
Peak
0.
RO
RO
RO
RO
RO
0.
RO
0.
RO
RO
RO
RO
RO
RO
RO
RO
RO
RO
RO
RO
RO
RO
65-0.89
1
0
0
0
0
.06
.62
.61
.44
.63
2
1
1
0
4
0
.80
.08
.66
.65
.92
.00
65-0.89
0
0
0
0
0
0
.94
.72
.75
.74 10,
.73
.65
10,
4
96
32
273
90
12
493
TCD:
.84
.95 40.55
.13 13.82
.50 4,383.13
.42 38,01
.69
.00
65-0.89
1
0
1
5
1
2
0
0
0
0
1
1
0
1
1
2
.81
.75
.52
.38
.02
.08
.8«
.20
.97
.42
.19
.22
.36
.13
.62
.39
i
i
0
1
1
0
10
2
3
0
0
1
0
1
0
0
10
.31
,00
.74
.35
,15
.67
.54 4.87
.23
.06
.89
.64
.15
.74
.11
.83
.81
.54
0.828-1.139
0
0
0
0
1
.000
.831
.861
.947
.002 2378-TCDF AN
0.936-1.064
0
56.40 0
18.31 0
5,890.37 1
52.41 1
1
.000
.939
.973
.000 13C12-2378-TCDF ISO
.030
.128
0.846-1.085
0
0
0
0
0
0
5.67 0
1
1
1
1
1
1
1
1
1
.000
.911
.940
.951
.960
.971
.985
.000 2378-TCDD AN
.011
.040
.047
.053
.081
.085
.089
.095
0.878-1.122
DC
DC
NL
SN
2
0:00
15:00
16:25
16:39
Peaks
4
4
0
4
,230
2
,234
.52
.33 4.33
.06 4,230.06
.66
.39
0
0
1
1
.000
.914
.000 37C1-TCDD SUR1
.014
Triangle Laboratories, Inc.® Analytical Services Division
801 CapHote Drive • Durham, North Carolina 27713
Phone: (919) 544-5729 • Fax: (919) 544-5491
Printed: 15:55 11/11/96-.
3
-------
Page No. 2
11/11/96
Compound/
M_Z.... QC.Log Omit Why
13C12-TCDD
Listing of T966616B.dbf
Matched GC Peaks / Ratio / Ret. Time
,.RT. OK Ratio Total.Area... Area.Peak.1.. Area.Peak.2.. Rel.RT Compound.Name.. ID..
0.65-0.89
0.878-1.122
332-334
N
332-334
PeCDF
340-342
340-342
13C12 -PeCDF
352-354
352-354
PeCDD
356-358
DC
DC
DC
DC
DC
DC
DC
DC
DC
DC
DC
DC
DC
DC
DC
DC
DC
DC
DC
DC
DC
DC
DC
DC
DC
DC
DC
DC
DC
NL
SN
4
NL
SN
SN
SN
SN
SN
SN
SN
SN
SN
SN
SN
SN
SN
SN
SN
SN
SN
WH
0
NL
5
NL
SN
SN
SN
SN
SN
SN
0:00
15:12
16:10
16:25
16:38
16:49
Peaks
0:00
17:52
19:47
19:55
20:05
20:09
20:23
20:51
20:59
21:11
21:15
21:38
21:44
21:48
21:56
22:30
22:47
23:05
23:20
Peaks
0:00
19:42
20:26
20:53
21:17
21:52
Peaks
0:00
19:52
20:24
20:40
20:57
21:07
21:18
RO
RO
1.
RO
RO
RO
RO
RO
RO
RO
RO
RO
RO
RO
RO
RO
RO
RO
RO
RO
RO
RO
1,
RO
RO
RO
1
RO
RO
RO
RO
RO
RO
RO
2
0
0
0
0
0
.71
.87
.81 4
.79 8
.29
.73
13
Jl "U,—.. .... .
32-1.78
0
1
1
0
0
0
1
0
0
0
0
4
0
0
2
0
3
0
0
,32
0
1
2
1
1
I
.32
2
3
1
0
0
1
0
.47
.03
.90
.46
.56
.84
.94
.39
.08
.13
.97
.14
.37
.42
.15
.66
.15
.63
.75
-1.78
.54
.68
.00
.45 8
.24
.46 4
12
-1.78
.04
.35
.81
.68
.60
.14
.98
3
42
,989
,182
5
84
.96
.73 19.84
.42 2,227.76
.04 3,598,60
.62
.44 35.77
0
22.89 0
2,761.66 0
4,583.44 1
1
48.67 1
.000
.926
.985 13C12-1234-TCDD
.000 13C12-2378-TCDD
.013
.024
RSI
IS1
,2S8.63
T?CDD / P0CDP Poiiows ** —
i
i
4
1
0
0
1
0
0
0
1
0
0
1
2
1
1
0
0
0
.25
.30
.31
.18
.53
.68
.60
.92
.25
.14
.64
.89
.46
.17
.19
.61
.00
.61
.63
.00
0.855-1.111
0
0
0
0
0
0
0
0
1
1
1
1
1
1
1
1
1
1
1
.000
.856
.947
.954
.962
.965
.976
.998
.005
.014
.018
.036
.041
.044
.050
.077
.091
.105
.117
0.808-1.192
0
72
11
,059
22
,208
.73
.98 45.71
.89 9.33
.24 4,775.80
.79 13.85
.28 2,500.79
0
27.27 0
4.66 0
3,283.44 1
11.17 1
1,707.49 1
.000
.943
.978
.000 13C12-PeCDP 123
.019
.047 13C12-PeCDF 234
IS2
SUR2
,375.18
PeCDF / PoCBD Fo X lows — —
i
0
1
0
1
1
0
.17
.79
.10
.91
.17
.24
.66
0.885-1.034
0
0
0
0
0
0
0
.000
.890
.913
.925
.938
.946
.954
Triangle Laboratories, Inc.® Analytical Services Division
801 Capitals Drive • Durham, North Carolina 27713
Phone: (919) 544-5729 • Fax: (919) 544-5491
Printed: 15:55 11/11/96
3:
-------
Page No,
11/11/96
Listing of 1-9666168.dbf
Matched GC Peaks / Ratio / Ret. Time
Compound/
M_2.... QC.Log Omit Why ..RT. OK Ratio Total.Area... Area.Peak.1.. Area.Peak.2-. Rel.RT Compound.Name.. ID.
356-358
13C12-PeCDD
368-370
368-370
HxCDF
374-376
K
374-376
13C12-HXCDF
384-386
384-386
DC
DC
DC
DC
DC
DC
DC
DC
DC
DC
DC
DC
DC
DC
DC
DC
DC
DC
DC
DC
DC
DC
DC
DC
DC
DC
DC
DC
SN
SN
SN
SN
SN
SN
SN
SN
SN
SN
WH
WH
WH
0
NL
2
NL
SN
SN
SN
SN
SN
SN
SN
SN
WH
m
KH
1
NL
SN
6
21:22
21:30
21:35
21:48
22:17
22:21
22:25
22:31
22:39
22:43
23:09
23:21
23:23
Peaks
0:00
22:20
22:30
Peaks
0:00
24:18
24:31
25:11
25:16
25:51
25:58
26:27
26:45
26:55
26:58
27:02
27:11
Peak
0:00
24:07
24:17
25:15
25:21
25:56
26:11
26:41
RO
RO
RO
RO
RO
RO
RO
RO
RO
RO
RO
RO
1.
RO
0.
0.
2.
1.
0.
3.
1.
2.
0.
1.
2.
0.
0.
89
84
47
31
45
26
39
19
85
79
58
92
23
0.
1.
0.
1.
0.
1.
2.
1.
0.
1.
0.
0.
0.
0.
89
33
92
66
48
28
08
22
85
33
79
99
39
00
32-1.78
19.67
1.52
1.43
1,
RO
RO
RO
RO
RO
RO
RO
RO
RO
0.
RO
RO
X l**ii m
05-1.43
1
0
1
0
0
1
1
0
0
0
1
1
3
.21
.41
.16
.78
.19
.13
.39
.61
.76
.45
.73
.52
.60
0.15
4,517.21 2,723.38
439.49 258.82
0.957
0.
0.
0.
0.
1.
1.
1.
1.
1.
1.
1.
1.
963
966
976
998
001 12378-PeCDD
004
008
014
017
037
046
047
AN
0.821-1.179
0.000
1,793.83 1.000 13C12-P6CDD 123
IS3
180.67 1.007
4,956.70
2.17
0.67
0
0
0
0
7
1
0
0
0
0
0
7
.97
.56
.61
.83
.28 4.24
.23
.47
.33
.34
.94
.34
.28
.43-0.59
1
0
0
0
0
0
0
0
.69
.52
.55
.50
.49
.50
.31
.50
Peaks
1
23
32
3,140
5,769
3,293
4
2,214
14,474
.79
.35 8.03
.17 11.37
.54 1,045.90
.79 1,909.60
.80 1,103.24
.87
.79 741.54
.44
0.945-1,063
0
0
.000
.959
0.967
0
0
1
3.04 1
1
1
1
1
1
1
.993
.997 123478-HxCDF
.020
.024 234678-HXCDF
,043
.055
.062
.064
.066
.072
AN
AN
0.842-1.158
0
15.32 0
20.80 0
2,094.64 0
3,860.19 1
2,190.56 1
1
1,473.25 1
.000
.951
.958
.996 13C12-HXCDF 478
.000 13C12-HXCDF 678
.023 13C12-HXCDF 234
.033
.053 13C12-HXCDF 789
SUR3
IS4
ALT2
ALT1
Above: HxCDF / HxCDD Follows
Triangle Laboratories, Inc.® Analytical Services Division
801 Capitola Drive • Durham, North Carolina 27713
Phone: (919) 544-5729 • Fax: (919) 544-5491
Printed: 15:55 11/11/96
33
-------
Page No.
11/11/96
Listing of T966616B.db£
Matched GC Peaks / Ratio / Ret. Time
Compound/
M_Z.... QC.Log Omit Why ..RT. OK Ratio Total.Area... Area.Peak.1.. Area.Peak.2.. Rel.RT Compound.Name.. ID.
HXCDD
390-392
390-392
13C12 -HXCDD
402-404
402-404
HpCDF
408-410
408-410
13C12 -HpCDF
418-420
418-420
HpCDD
424-426
424-426
DC
DC
DC
NL
WH
WH
0
0:00
26:41
26:45
Peaks
1.
RO
RO
RO
05-1.43
0.
2.
0.
1. OS-
DC
DC
DC
DC
DC
DC
DC
DC
DC
DC
DC
DC
DC
DC
DC
DC
DC
DC
DC
DC
DC
DC
NL
4
NL
SN
SN
SN
SN
SN
SN
SN
SN
SN
SN
WH
WH
0
NL
2
NL
SN
SN
SN
WH
WH
WH
0
0:00
25:32
26:06
26:11
26:30
Peaks
0:00
28:20
28:25
28:28
28:42
28:48
28:57
29:01
29:06
29:41
29:45
29:53
29:57
Peaks
0:00
28:19
29:36
Peaks
0:00
28:37
29:10
29:17
29:34
29:39
29:42
Peaks
RO
0,
RO
RO
RO
RO
RO
RO
RO
RO
RO
RO
RO
RO
0
RO
0
RO
RO
RO
RO
RO
RO
RO
1.
0.
1.
1.
1.
.88-
0.
0.
1.
1.
0.
1.
0.
1.
0.
0.
4.
0.
6.
73
55
85
1.43
41
96
19
21
20
- Above:
1.20
82
89
33
73
56
89
56
58
73
66
22
44
73
2.
1.
1.
0.
31
05
00
00
0.939
0
1
1
-1.017
.000
.019
.022
0.962-1.038
3.
12.
2,219.
4,744.
2,896.
9,872.
HxCDD
16
50 6.91
01 1,204.07
41 2,597.81
86. 1,578.65
78
/ llwTMir t^f-O T r\\ t«s
0
7.22 0
1,014.94 0
2,146.60 1
1,318.21 1
.000
.975
.997 13C12-HXCOD 478
.000 13C12 -HxCDD 678
.012 13C12-HXCDD 789
SUR4
IS5
RS2
0.995-1.051 '
1.
3.
0.
0.
1.
0.
0.
1.
0.
1.
0.
0.
0.
0.
48
20
74
45
31
37
75
57
43
20
47
61
22
00
.37-0.51
0.
0.
0.
.88-
68
41
.41
-1.20
1.50
1.36
0.40
1.53
3.74
3.25
0.44
3.
3,428.
931.
81
50 994.38
85 268.84
0
1
1
1
1
1
1
1
1
1
1
1
1
.000
.001 1234678-HpCDF
.004
.005
.014
.017
.022
.025
.028
.048
.051
.055
.058
AN
0.929-1.141
0
2,434.12 1
663.01 1
.000
.000 13C12-HpCDF 678
.045 13C12 -HpCDF 789
IS6
SUR5
4,360.35
; HpCDF / HpCDD Foliows —
0.
2.
1.
2.
0.
0.
94
61
57
00
96
49
0.53
0.
00
0.973-1.006
0
0
0
1
1
1
1
.000
.978
.997
.001 1234678-HpCDD
.010
.013
.015
AN
13C12-HpCDD
436-438
DC HL
0.88-1.20
0:00 RO 1.66
3.00
0.966-1.034
0.000
Triangle Laboratories, Inc.® Analytical Services Division
801 Capftola Drive * Durham, North Carolina 27713
Phone: (919) 544-5729 • Fax: (919) 544-5491
Printed: 15:55 11/11/96,
-------
Page No.
11/11/96
Listing of T966616B.dbf
Matched GC Peaks / Ratio / Ret. Time
compound/
H_Z.... QC.Log Omit Why .,RT. OK Ratio Total.Area... Area.Peak.1.. Area.Peak.2.. Rel.RT Compound.Name.. ID.,
436-438
28:38 1.06 12.74
29:16 1.03 3,359.52
DC SN 29:37 RO 0.79 2.93
2 Peaks 3,372.26
6.55 6.19 0.978
l',702.30 1,657.22 1.000 13C12-HpCDD 678 IS7
1.012
Above: HpCDD / Octa-CDD and CDF Follows
OCDF
442-444
442-444
DC NL 0:00
0.76-1.02
0.80
DC SN 29:15 RO 0.54
0 Peaks
2.59
1.06
0.00
0.874-1.126
0.000
0.922
OCDD
458-460
458-460
0.76-1.02
DC NL 0:00 RO 0.42
DC SN 31:45 0.94
0 Peaks
0.70
1.73
0.00
0.874-1.126
0.000
1.001 OCDD
AN
13C12-OCDD 0.76-1.02
470-472 DC NL 0:00 RO 10.67 0.06
31:43 0.88 3,4S9.9S
470-472 1 Peak 3,459.96
1,624.25
0.995-1.006
0.000
1,835.71 1.000 13C12-OCDD
IS8
Column Description "Why" Code Description QC Log Desc.
M_2 -Nominal Ion Mass(as)
..RT. -Retention Time (inm:ss)
Rat.l -Ratio of M/M+2 Ions
OK -RO=Ratio Outside Limits
Rel.RT-Relative Retention Time
End of Report
WL-Below Retention Time Window
WH-Above Retention Time Window
SN-Below Signal to Noise Level
-------
File:T966616 #1-835 Aaq:l-NOV-96 11:44:10 EI+ Voltage SIX 70T lfoi.fle.-838
303..9016 Tt2 BSUa(2S6,30,-3.Q) PKD(S,3,lr0.10\,3352.0,Q.QO*rF,F) Exp:EPCUS
TRIANGLE LABS Text-.TLI M23 BLANK TLI&39291R1 JWJ. TIME - 11s 46
100* A7.16E3
13:00 14:00 15:00
File:T96S616 #1-835 ,Scg-,-l-.iroV-96 11:44:10 EI+ Voltage
305.8987 Fs2 BSUB(256,30, -3.0) PJO>(5,3,1, C.10%,315.2. 0
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315.9419 F:2 SSUB(256,30,-3.0) PJOJ(5,3,1,0.10*, 5140.0,
TRIANGLE LABS Text .-HI M23 BMTOT TEI#352S1H1
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TRIANGLE LABS Texts III K23 BiaWK HJWSiSlSl
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TRIANGLE LABS TextiTLI M23 BLANK TLI#39291R1
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0:
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375.8364 F:2 Exp:EPCOS
TSIANGLE LABS TextsTLI M23 BLANK TLI#39291S1
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15:29
I
16:00
SIK 70T
17:00
18:00
8E7
1E7
4E7
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Time
JKT. TIME - 11:46
- i I5..J5
13-00
14-00
15:00
42
-------
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19.8965 Fs2 BSUB(2S6,30, -3. 0) PKD(5,3rl, 0.10%,2688.0,0.00%,F,F} ExpsEPCUS
TRIANSLE LABS TextiXLI M23 BLANK TLI#39291Sl IK7. TIME - 11:46
001 A4. 9E4
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FilesT966616 #1-835 Acq:l-NOV-9S 11:44:10 EH- Voltage SIX 70T No±Be:369
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TRIANSLE LABS TextsTLI H23 BLANK TLI#39291R1 IK7. TIME - 11:46
1003s AS.
80J
a7,58E3
A5-78EA34.23E.^-^
A4.87E4
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18:00
18:00
18:06
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12.126
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L7.6E6
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14:00 15:00 16:00 17:00
FileiT9666ie #1-835 Acq:l-NOV-96 11:44:10 EH- Voltage SIS 70T Noiae:3035
331.9368 F:2 BSUB(256,30, -3.0) PKD(5,3,1,0.101,12140.0, 0.00*,F,F) ExpsEPCUS
TSIAKSLE LABS Text:Til M23 BLANK TLX#39291X1 IWT. TIME « 11:46
1003i A3.J
80:
60:
40:
A2.23E7
14:00 15:00 16:00 17:00
rile:T966616 #1-835 Acq:l-NOV-96 11:44:10 EH- Voltage SIM 70T Koiaesll22
333.9338 Fs2 BSUB(256r 30, -3. 0) PKD(5,3,1, 0.10%,448S. 0,0, 00%,F,F) Exp:EPCUS
TRIANGLE LABS Text-.TLI M23 BLANK TLI#39291R1 IKT. TIME - 11:46
100* A4.58E7
60:
40:
20:
0.
A2.76E7
14:00 15:00 16:00 17:00
JFilesT966616 #1-835 Acysl-NOV-96 11:44:10 EH- Voltage SIX 70T Noiaes259
327.8847 Fi2 BSUB(256,30, -3.0) PKD(5,3,1, 0.101,1036.0, 0.00%,FrF) Exp:EPCUS
TRIANGLE LABS TextiTLI M23 BLANK TLH39291R1 INJ. TIME = 11:46
1003j 'A4.23E7
so:
so:
40:
20:
0J
14100
FilesT966SlS #1-835
330.S792 F:2 ExpsSPCUS
TRIANGLE LABS TextsTLI M23 BLANK
100S
80:
60:
40:
20:
.0:
15:00 16:00
-SOV-96 11:44:10 EH- Voltage SIS 70T
17:00
TLI#39291X1
ISJ-. TIME - 11:46
14. -00
15:00
isoo
17:00
-------
File:T966616 #1-835 Acq:l-NOV-96 11:44:10 EX+ Voltage SIS JOT Noiae:381
33S.S597 Fi2 BSU3(256,30, -3.0) fKD(5,3,l, 0 .101,1524 . 0, 0 , 00%, F,F) Exp-.EPCUS
TRIANGLE LABS Teit:TLI M23 BLANK TLI#39291R1 JKT. TIKE =• 11:46
1001 Al - SE4
18:00 19:00 20:00 21:00 22:00
File:T966616 11-835 Acq:l-NOV-96 ll:44s!0 EH- Voltage SIS 70T Noiae:807
341.8567 F:2 BSUB(256,30,-3.0) J>XDf5,3,l,0,10%,3228. 0,0, 00%,F,F) BfptEPCOS
TRIANGLE LABS Text-.TLI M23 BLANK TLI#39291R1 INJ. TIME = 11:46
18:00 19:00 20:00 21:00 22:00
File:T966616 #1-835 Acq:l-NOV-96 11:44:10 EI+ Voltage SIS 70T No±se:221
351.9000 F:2 BSUS(256,30, -3.0) PKD(5,3,1, 0.10%, B84.0, 0.00*,F,F) Exp:EPCUS
TRIANGLE LABS Text:TLI M23 BLANK TLI#39291R1 UKT. TIME = 11:46
1001 A4.78E7
S'iF") A1.40E4
' /9.29E3A
1003
401
201
0.
Al. 69E4
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23:00
A1.23E4
23:00
802
sol
401
201
0.
A2.50E7
18:00 19:00 20:00 21:00 22:00
File:T96661S #1-835 Acq-.l-NOV-96 11:44:10 EH- Voltage SIR 70T Soises410
353.8970 F:2 BSUB(256, 30, -3 . 0) PKD(5,3,1,Q. 10*, 1640.0,0 ,OOl,F,F) ExptEPCVS
TRIANGLE LABS Text-.TZI M23 BLANK TLI#39291R1 ISJ. TIME = lls
1003
80:
23:00
60:
40:
20:
o.
Al. 71E7
18:00 19:00 20:00 21:00
F±le:T966616 #1-835 Acq:l-NOV-96 11:44:10 EI+ Voltage SIR 70T
330.9792 F:2
TRIANGLE LABS Teit:TLI M23 BLANK
100*
22:00
23:00
18:00 19:00 20:00 21:00
File:T966616 #1-835 Acqsl-NOV-96 11:44:10 EI+ Voltage SIR 70T
409.7974 F:2 ExptEPOJS
22:00
23:00
TRIANGLE LABS
100*
so:
so:
40:
20:
0:
18:
ii
18.-00
Teit:TLI If23 BLANK
19:28
TLI#39291R1
30,31 20:54
ISJ. TIMS =
21 46
21:31
21:201
11:46
.1. OE4
.8.2E3
.6.2E3
.4.1E3
.2.1E3
.O.OEO
Time
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.9.1E6
.6.8E6
.4.SE6
.2.3E6
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Time
.7.9E6
.6.3E6
.4.7E6
.3. 1E6
.1. 6E6
.O.OEO
riffle
20; 00
21:00
22:00
-------
•ile.-r3ggS.lt> H-B3S Acq:l-NOV-96 11:44:10"jfeff VolCage slM 70T tfoiaei472
55.8546 F:2 BSOB(256,30, -3.0) PKD(5,3,1,0,101,1$$8.0,0.00*,F,F) ExpiEPCttS
TRIANGLE LASS TexttTLI M23 BLANK TLI#39291K1 1KT. TIME • 11:46
1004 A2.07E4
JO.-00 21:00 22s00
FilesT966616 #1-835 Acq:l-NOV-96 11:44:10 EH- Voltagre SIR 70T Noiae:228
357.8516 F:2 BSm(256,30, -3. 0) P1O>(5,3,1,0.101,912.0, 0,00*,F,F) £xp:EPCUS
TSIANSLE LABS Teit:TLI M23 BLANK TLIt39291Rl IKT. TIME -
100^
A4.27E3 A5.70E3
A8.42E3 AS.5SE3A7.74E3
A4.10E3
80_
SO.
40,
20.
23:00
6E4
20:00 21:00 22:00
File:T9S661S #1-835 Acqil-NOV-96 11:44:10 EH- Voltage SIR 70T Jfoise:5fl9
367.8949 F:2 BSUB(256,30, -3 . 0) PtX>(5,3,1, 0.10^,2356. 0, 0. 00\,F,F) Exp:EPCUS
TRIANGLE LABS Text:TLI H23 BLANK TLI#39291R1 XW. TIME - 11:46
1004 . A2.72E7
80.
so:
401
20'.
23:00
0.
2.59E6
20:00 21:00 22:00
F±le:T966616 #1-835 Ac
-------
File:TS66616 #1-505 Acgsl-NOV-96 11:44:10 EI+ Voltage SIS 70T NoiseiSSS
373.8208 Fs3 SSUS(256,30,-3.0) PKD(5r 3,1,0.10^,2380.0,0. OQ*,3?,T) ExpsEPCUS
TSIANSLE LASS TextiTLI M23 BUM* TLI#39291R1 ZKT. TIMS = II.- 46
1004 A4.24E4
24': 00 25:00 26:00
File: fa 66616 #1-505 Acq:l-NOV-96 Ili44tl0 EI+ Voltage SIS 70T Noiae:488
375.8178 F:3 BSUB(256,30, -3.0) PKD(5,3,1, 0.101,1952. 0,0. OQ*,F,F) ExpiEPCUS
TRIANGLE LASS Teit:TLI M23 BLANK TLI#39291R1 JKT. TIME - 11:46
24i00 25:00 26:00
File:T966616 #1-505 Acq:l-NOV-96 11:44:10 EI+ Voltage SIS 70T Noise:998
383,8639 F:3 SSUB(256,30,-3.0} PKB(5,3,1,0. J0%,3992. 0,0. 00\,P,F) Exp;EPCUS
TRIANGLE LABS Text.-lZJ H23 BLANK TLH39291S1 JKT. TIME =• 11:46
100S,
Al.84E3
A6.S5E3 A2.55E3
27: 00
27:00
100*
40.
201
0.
24:00 25:00 26:00
F±le:T966616 #1-505 Acq:l-NOV-96 11:44:10 EI+ Voltage SIS 70T
445.7555 F:3 Exp:EPCOS
TRIANGLE LABS Text:TLI M23 BLANK TLIX39291R1 INJT. TIME =
100% 26 08
24:20
27:00
11:46
40.;
20.
0^
26:23
26156
KJ-
ft
rt
/v
r^i /
A1.10E7
ft i
A A7.42S6
\ ^
I A /f
4:00 25:00 26:00
•.T966616 #1-505 Acq:l-NOV-96 11:44:10 EI+ Voltage SIX 70T Noiae:589
8610 F:3 BSUB(256, 30, -3 .0) PKD(5,3,1,0.10%,2356.0,0.00*,F,F) Exp:EPCUS
U3GLE LABS Text:TLI M23 BLANK TLI#39291Xl JKT. TIME = 11:46
A3
A
IV
)6£7
A2.19E7
"/
/
>4} 00 25:00 26:00
• :T966616 #1-505 Acq:l-NOV-96 11:44:10 EI+ Voltage SIR 70T
9760 F:3 ExpsEPCUS
UtSLX LABS Text:TLI M23 BLANK TLI#39291X1 INJ~. TIME = 11:46
L^, 24:20 24:40 24:5625: 07 25:19 25-30 25-49 26:1526:26 26-
v\^v^_^^A«_rAVAA»^^^xx~%-*^.-^A-*>'JVv\ A/v\r -- '^/S — *?-•*" _r.-'i~r — »^_^v»i . _/\~ » .if J
^
^ "
27:00
\7E7
V
27:00
f026j5l27:02
^•VMN»vSrfV/v-«AAA.
w
i 07
24 .* 00
25:00
26:00
27:00
.O.OEO
Time
,5. 7E6
.4.5E6
.3. 4E6
,2. 3E6
.1. 1E6
O.OEO
Time
,1. 1E7
9.0E6
6.7E6
4.5E6
2.2E6
O.OEO
Time
.1.6E7
.1.3E7
.9. SE6
6.4E6
.3.2E6
.O.OEO
Time
.8.3E3
.6.7E3
.5,OE3
.3. 3E3
.1. 7S3
.o.oso
Time
-------
'UestaSSSIS il-SOS Acq-.r-XOV-aS lltMUO Sl+ Voltage 4lJt 70T NoiseiS41
89.8156 F:3 BSUB(256,30,-3,0) PKD(5, 3,1, 0.101,2564.0,0.00\,F,f) ExptEPCUS
TRIANGLE LABS TtortsTLI M23 BiAMT TLI#33291K1 JKT. TIME - 11:46
00* A4 . SE3
24:36 24:48 25:00 25:12 25:24 25:36 25:48 26:00 26:12 26:24 26:36 26:48
file:T96661S #1-505 Acq:l-KOV-96 11:44:10 EI+ Voltage SIS 7QT Soiae:873
391.8127 f:3 SSWe(256f 30, -3. 0) PXS(S,3,1,0.10%, 3492,0,0. 00*,?,f) Exp:EPCVS
TRIANGLE LABS TextiTLI M23 BLANK TLH39291R1 HfJ". TIME - 11:4 6
IOCS
24:36 24:48 25:00 25:12 25:24 25:36 25:48 26:00 26:12 26:24
File:T966616 41-505 Acq:l-NOV-96 11:44:10 EI+ Voltage SIB 702* Noise:923
401.8558 Fs3 BStm(256,30, -3.0) PXS(5,3,1, 0. J0%, 3692. 0,0,00%,F,F) ExptEPCUS
TXIAMGLE LABS TertiTZI M23 BiMHf TLI#39291S1 IJKJ. TIME = 11:46
1004 A2.&OE7
26:36 26:48
so:
601
40:
20:
A1.58E7
24:36 24:48 25:00 25:12 25:24 25:36 25:48 26:00 26:12 26:24 26:36 26:48
PiletT966616 #1-505 Mcqil-NOV-96 11:44:10 Eli- Voltage SIX 70T Koiae:653
403.8529 F:3 BSUB(256, 30, -3. 0) PKD(5,3,1, 0.101,2612.0,0. OOl,P,f) Exp:EPCUS
TRIANGLE LABS TsxtsTLI M23 SLASK TLlt39291Zl JKT. TIME - Ils46
100% A2.15E7
801
60.
401
201
Al.32E7
24:36 24:48 25:00 25:12 25:24 25:36 25:48 26:00
r±lesN66616 #1~505 Acqil-NOV-96 11:44:10 EI+ Voltage SIR 70T
392.9760 f:3 Exp:EPCUS
TRIANGLE LABS T&rtsTLI M23 BLANK TLI039291X1 INJ'.
26:12 26:24 26:36 26:48
TIME -
1.3E4
1.0E4
7.7E3
.S.1E3
.2.6E3
O.OEO
Time
1003
801
601
401
201
24:40
26s 51
7.9E6
.6.3E6
.4.7E6
.3 , 2E6
1.6E6
.O.OEO
TJJS>
.6.5E6
.5.2E6
.3. 9E6
.2. 6E6
.1.3E6
.O.OEO
Tine
.1. 6E7
.1. 3E7
.9.4E6
.6.3E6
.3.1E6
.O.OEO
24:36 24:48 25:00 25:12 25s24 25:36 25:48 26:00 26:12 26:24 26:36 26:48
-------
File:T966616 #1-443 Acq:l~NOV-96 11:44:10 EI+ Voltage SIS 7QT Noises376
407.7818 Ft4 BStm(256, 30,-3.0) PKD( 5, 3,1, 0.101,1504. 0,0. 00*,F,F) Exp:EPCUS
TRIANGLE LABS TextsTLI M23 BLANK TLIt39291Sl IW. TIME " 11:46
1004
28i24 28:36 28:48 29:00 29:12 29:24 25:35 29.-4S
Fi-Ze.-T956616 #1-443 Acq:l-NOV-96 11:44:10 EI+ Voltage SIS 70T Nd±ae:898
417.8253 F:4 BSUB(256, 30, -3.0) PKD(5,3,1, 0,10*,3592.0,0, 00%,F,F) ExpsEPCUS
TRIANGLE LABS Text:TLI M23 BLANK TLI#39291X1 ItKT. TIME = 11:46
100J
80:
28il2 2S;24 28:36 28:48 29:00 29:12 29:24 29:36
File:T966616 #1-443 Acq:l-NOV-96 11:44:10 EI+ Voltage SIS 70T Htoise:458
409.7789 F:4 BSUB(256r30, -3. 0) PKD(5,3,1, C.10%,1832. 0,0.00%,F,F> ExpsEPCUS
TRIANGLE LABS Text: III M23 BLANK TLH392S1S1 XWJ. TIME = 11s 46
1003.
ao":
60:
29s 48
3000
40:
20:
A1.69E4
A4.31E3
A6.77E3 A3.03E3
A1.29E4
Al , 02E4
JO: 00
60:
40:
20:
o
A2 . 69ES
28:12 28:24 28:36 28:48 29:00 29:12 29:24 291:36 29:48
File:T966616 #1-443 Acq:l-NOV-96 11:44:10 EI+ Voltage SIS 70T Noise:131B \
419.8220 F:4 BSVB{256, 30,-3.0 ) PKD(5,3,1, 0.10^,5272. 0,0. 00%, F, F) ExpsEPCUSi
TRIANGLE LABS Text:HI H33 BLANK TLIt39291Sl ItKT. TIME = 11:46
1003
aol
60:
40:
20":
o:
A2.43E7
I
A6.63E6
28:12 28:24 28:36 28:48 29:00 29:12 29:24
file:T966616 #1-443 Acq:l-NOV-96 11:44:10 EI+ Voltage SIS 70T
430.9729 F:4 Ezp:EPCUS
TRIANGLE LABS Text:TLI M23 BLANK TLH39291S1 ItKT. TIME
1°°* 28:21 . 28:29 28.-3S -28:49
80:
60:
40:
2Ss36
2948
:45
28:12 28:24 28:36 28:48 29:00 29:12 25:24 2S.-36
File:T966616 #1-443 Acq:l-NOV-96 11:44:10 EI+ Voltage SIS 70T
479,7165 F:4 ExpiSPCUS
TSIANGLE LABS Text:TLI M23 BLANK TLH39291S1 HKT. TIME = 11:46
1004
29:48
O: DC
30:00
.1. 1E5
.8.7E4
.6.5S4
.4.3E4
.2.2E4
.0.020
Time
4.4E4
.3.5E4
.2.6E4
.1. 7E4
.8.7E3
O.OEO
Tiae
.3.3E6
.2. 7E6
.2.0E6
.1.3E6
.6.6E5
.O.OEO
Tine
.7.926
.6.3E6
.4. 7E6
.3.2E6
.1. 6E6
T_UB
-------
il-443 Aaq:l-lfov-se lli4i:IV Et+ Voltage SI* 70T'XaIsBs347
'•23.7766 ri4 BSUS(256,30, -3. 0) PKD(5,3,1, 0.10%,1388.0, 0. 00%,r,F) ExpsEPCUS
TRIANGLE L&BS XextiTLI M23 BLANK TLI039291R1 IMT. TIMS - 11:46
IOCS A1.50E4
28:30 28:36 28:42 28:48 28:54 29:00 29:06 29:12 29:18 29:24 29:30 29:36
FilesT966616 #1-443 Rcqsl-SQV-96 11:44:10 Eli- Voltage SIR 70T Noige:229
425.7737 Fs4 BSUS(256,30,-3.0) ?KD(5,3,1, Q.10^,916.0,0.00\,T,W) Exp:EPCUS
TRIANGLE LABS TextiTLI M23 BLANK TLH39291R1 INJ". TIME = 11:46
100* Al. 03JE4
A7. 77E3
6.0S3
4.SE3
'.3. OE3
;i. 5E3
f.0. OEO
29:42 Time
28:30 28:36 28s42 28:48 28:54 29:00 29:06 29:12 29:18 29:24
rile:T966616 #1-443 Acq:l-NOV~96 11:44:10 EI+ Voltage SIS 70T Noise: 1219
435.8169 F:4 BSUB(2S6,30,-3.0) PKD(5,3,1,0.101,4876.0, 0. OOl,F,F) Exp-.EPCUS
TRIANGLE LABS Text .-HI M23 BLANK TLH39291S1 JMT. TIMS = 11:46
1003, A1.JOE7
so:
so:
40:
20:
29:30 29:36 29:42
6.4E6
-5.1E6
.3.9E6
'-2,6E6
'.1 . 3E6
28:30 28:36 28:42 28:48 28:54 29:00 29:06 29:12 29:18 29:24
File:T966616 tl-443 Acq:l-JTOV-96 11:44:10 EI+. Voltage SIS 70T Soiae: 737
437.8140 F:4 BSUB(256r30,-3.0) PKD(5,3,1, 0.101,2948. 0, 0.00%,F,F; Exp-.EPCUS
TRIANGLE LABS Tezt:XLI M23 BLANK TLH39291S1 ISJ'. TIME = 11:46
1004 Al. 66E7
so:
60:
40:
20:
29:30 29:36 29:42
Time
,5.0E6
.3. 7E6
-2.SE6
'.1.2E6
I I 1 I i I I I I I i i I I I i 1 I i I f f ! i I""*1 j 1 1 I 1 i""!' 1 i 'T I "i ( I < ) I 1 j'lrfi i I t I 1 I f 1 I" I ( 1 I 1 1 t I i i I '! "I I 1 \ 1 I 1 I I I
28:30 28:3S 28:42 28:48 28:54 29:00 29:06 29:12 29:18 29:24 29:30 29:36 29:42
O.OEO
FilejT9SSS15 #1-443 Acqsl-SOV-96 11:44:10
430.9729 F.-4 ExpsEPOJS
TRIANGLE LABS TexttTLI M23 BLANK TLIt39291Sl
Voltage SIM 70T
1003
so:
60:
40:
20:
28:36
1K7. TIME - 11:46
29:17 29:23
29:37,
-1.1E7
.9. OE6
.6.BE6
.4.5X6
.2.3E6
.y.i;.,,! nM-y-,, , .yi.i.-.i, f ., .^•lyim. f ,,,,.(—!!..,; . ,, mjmi^.fm.fmum, , , ,,-^111, . , ,.1^1.1.1;-;. pym,^ f-fm^mm...:^ | i ( ! I 1 ( ( |"|^""T f'"'t ' t t 1 ^y""f T'[ T I" I t I I •t'T"""*'
28:30 28:36 2«:42 28:48 28s54 29:00 29:06 29:12 29:18 29,-24 29:30 J9:36 29:42
O.OEO
?!*<
-------
File:T966616 #1-443 Acqrsl-WOV-96 ll.-44:10 EH- Voltagre SIX 70T NO3.ae:577
441.7428 F:4 BSOB(256, 30,-3,0) PXD{7,2,3f0.10*,230B.O,0.00%,r,F) Exp:EPCUS
TRIANGLE LABS TextsTLI H23 BLAKK TLI#39291X1 IJKT. TIMS - 11:46
1COJ
SOJ
80J
701
601
501
401
301
201
101
01
29:00 30:00 31:00 32:00
File:T966616 #1-443 Acq:l-SOV-96 11:44:10 EI+ Voltagre SIX 7037 Noises 719
443.7399 F:4 SSOB(256,30, -3.0) PXD( 7,2,3,0.101,2876. 0, O.QQ*rF, T) Exp:EPCUS
TRIAHGLE IA3S TextiTZI M23 BIANK 1ZIt39291Sl IKJ. TIME - 11
1001
A4.94E3
A1.25E4
A7.87S3
Al.05E4
33:00
2.2E4
.2. OE4
.1. 8E4
.1. 5E4
.1. 3E4
1.1E4
.8.SE3
.S.6S3
4.4E3
.2.2E3
O.OEO
Time
46
29:00 30:00 31:00 32:00
File:TS66615 #1-443 Aeq:l-lfOV-96 11:44:10 EI+ Voltaye SIS 70T
430.9729 F:4 Exp:EPCUS
TSIANSLE LABS Teit:TZI M23 BLANK TLI '#39291X1 ISJ". TIME «
29:07 30:20 ifi.Ky 31:39 32:
28:21
33:00
11:45
29s00 30:00 31:00
File:T966616 #1-443 Acq>l-KOV-9S 11:44:10 EI+ Voltage SIS 70T
513.6775 F:4 Exp:EPCUS
32:00
33:00
TRIANGLE LABS
1003!
Text: TLI If 23 BLANK TLI#39291X1
29:54
J1KT. TIME "
11:
29:00
30tOO
31:00
32100
33:00
-------
'ile:T966616 #1-443 Acqil-HOV-96 11:44:10 EX+ Voltage SIS 70T Hoi.ae:167
457.7377 ft4 SSVS( 256,30, -3.0) fKD(7,2, 3,0,10%, 666. 0, 0.00*,F,F) Elp:EPCUS
TRIANGLE LABS TextiTLI M23 BIANK TLIH39291R1 I«T. TIMS = 11146
100*
32:06
31:36 31:42 31:48 31:54 32:00
File:T966616 #1-443 Aeq:l-mv-9S 11:44:10 EI+ Voltage SIR 70T Noi»e:392
459.7348 F:4 SSUB(256,3Q, -3. 0) PXD( 7,2,3,0. 10%,1SS8. 0,0.00\,f,f} ExpiEPCUS
TRIANGLE LABS TeXt:TLI M23 BISUUK TLX#39291R1 INJ. TIME = 11:46
1003:
80.
so:
401
20:
A8.44E3
r2.7E3
-2.2E3
'.1. 6E3
11.1E3
'.5.5E2
.O.OEO
32:12 Time
801
601
401
201
AB.92E3
1.3. 6E3
"-2.7E3
11. BE3
"-8.9E2
32:06
31:36 31:42 31:48 31:54 33:00
F±le:T966616 #1-443 Acq:l-KOV-S6 11:44 ilO EH- Voltage SZ8 70T Noiae:162
469.7773 F:4 BSUB(256,30,-3.0} PKD(7,2,3,0.10%,648.0,0.00%rFrF> Exp:EPCUS
TRIANGLE LABS Text .-III M23 BLANK TLI#39291R1 IK7. TIME = 11:46
100S A1.S2E7
a ol
601
401
201
O.OEO
32:12 Tims
-4 . 7E6
.3.5E6
-2.4E6
.1.2E6
32:06
31:36 31:42 31:48 31:54 32:00
File:T966616 #1-443 Acq:l-HOV-96 11:44:10 EI+ Voltage SIS. 70T SoiaeilS
471.7750 F:4 BSUS(256,30, -3.0) ?m(7,2,3,0,10\, 60.0,0.00\,frf) Ezp-.EFCUS
TRIANGLE LASS Text:TLI M23 BLANK H.I#39291R1 IMJ. TIME = 11:46
100$ A1.84E7
801
601
401
201
.O.OEO
32:12 Time
6.6E6
.5.3E6
.4.0E6
.2.6E6
-1.3E6
-O.OEO
31:36 31:42 31:48 31:54 32:00
File:T966616 #1-443 Acq:l-SOV-96 11:44:10 EI+ Voltage SIR 70T
430.9729 F:4 Exp:EPCUS
TRIANGLE LASS Text.:TLI K23 BLANK TZI439291R1 JJK7. TIMS
100S, 31139 31:42
32:06
32:12
Time
11:46
801
601
401
201
0.
31:52
32:01
32:09
1.1E7
-9.2E6
-6.9E6
.4 . 6E6
.2.3E6
31:36
31:42
31s4B
31:54
32:00
32:06
.O.OEO
32:12 Time
-------
Rtf , iass
Jkight 5,35yoLts Span
Systa fiU nate
Data f lit naie
itsdutlm
froupmber
hnizatton «de
%Uehii^
itf, lassss
« 2S3 J 331'
B 14 K 332
C 388 L "334
0 318 H 348
E 313 N 342
F 3cB 0 ^2
6 322 P 14
H 3E8 5 88
r 111 3 '*5
i *Vl ' F^'J
Channel I 338,3792
Height 5.29 mts Soan
p€»-.op
iip
JPCOS2
IM8 i
? i
Ci*
WLfflGE
416^68
S 368
" Tin
i J/B
U 37S
v 418
?SSR :CD
ii8 :ci3
-------
TLI Project: 39291rl
Client Sample: 23A-1
Method 23 PCDD/PCDF Analysis (a)
Analysis File: T966601
Client Project:
Sample Matrix:
TLI ID:
Sample Size:
Dry Weight:
GC Column:
Eastern Ridge Lime Facility
M23TRAIN Date Received: 10/19/96
143-23-lA,B Date Extracted: 10/21/96
Date Analyzed: 10/31/96
1.000 Dilution Factor: n/a
n/a Blank File: T966616
DB-5 Analyst: BB
Spike File:
ICal:
ConCal:
% Moisture:
% Lipid:
% Solids:
SPX23708
TF53286
T966598
n/a
n/a
n/a
2,3,7,8-TCDD
1,2,3,7,8-PeCDD
1,2,3,4,7,8-HxCDD
1,2,3,6,7,8-HxCDD
1,2,3,7,8,9-HxCDD
1,2,3,4,6,7,8-HpCDD
1,2,3,4,6,7,8,9-OCDD
2,3,7,8-TCDF
1,2,3,7,8-PeCDF
2,3,4,7,8-PeCDF
1,2,3,4,7,8-HxCDF
1,2,3,6,7,8-HxCDF
2,3,4,6,7,8-HxCDF
1,2,3,7,8,9-HxCDF
1,2,3,4,6,7,8-HpCDF
1,2,3,4,7,8,9-HpCDF
1,2,3,4,6,7,8,9-OCDF
Total TCDD
Total PeCDD
Total HxCDD
Total HpCDD
Total TCDF
Total PeCDF
Total HxCDF
Total HpCDF
ND
ND
ND
ND
EMPC
0.04
0.09
0.12
0.01
0,01
0.03
0.01
0.01
ND
0.04
ND
0.06
0.15
0.03
0.20
0,07
0.99
0.22
0.10
0.06
0.01
0.02
0.02
0.02
0.007
0.91
0.96
0.77
1.63
1.74
1.34
1.40
1.23
0.02
0.89
0.02
0.82
29:14
31:42
15:37
20:52
21:50
25:13
25:20
25:55 B_
28:18 H
31:46 ~~
3 0.17
1 0.12
2 0.20
2
12 1.0
6
5
3
—
Page 1 of2
X2J7J"SR vl.14, LARS 6.08.00
Triangle Laboratories, lnc.«
801 Capitola Drive • Durham, North Carolina 27713
Phone: (919) 544-5729 • Fax: (919) 544-5491
Printed: 16:0311/11/96
53
-------
TLI Project; 39291rl
Client Sample: 23A-1
Method 23 PCDD/PCDF Analysis (a)
Analysis File: T966601
Internal Standards
13Ci2-2,3,7,8-TCDF
13Ct2-2,3,7,8-TCDD
'3C12-l,2,3,7,8-PeCDF
13Ci2-l,2,3,7,8-PeCDD
13C,2-l,2,3t6,7,8-HxCDF
13Ct2-l,2,3,6,7,8-HxCDD
13e,2-l,2,3,4,6,7,8-HpCDF
13C12-1,2,3,4,6,7,8-HPCDD
1}CI2-1,2,3,4,6,7,8,9-OCDD
AmL (ngl
6.8
7.1
6.6
6.0
7.1
8.1
8.1
8.2
16.5
37ei4-2,3J,8-TCDD
13C12-2,3,4,7,8-PeCDF
13e,2-l,2,3,4,7,8-HxCDF
13d2-l,2,3,4,7,8-HxCDD
13Ci2-l,2,3,4,7,8,9-HpCDF
Alternate Standards (Typ» A>
13C,2-l,2,3,7,8,9-HxCDF
3Ci2-2,3,4,6,7,8-HxCDF
4.2
4.2
4.5
4.2
4.2
AmL (tig
4.4
4.4
13CI2-1,2,3,4-TCDD
13C12-l,2,3,7,8,9-HxCDD
%R«overy
85.0
88.5
83.1
75.6
89.2
102
101
102
103
105
106
113
104
105
%R«covety
109
109
QC Limits
40%-130%
40%-130%
40%-130%
40%-130%
40%-130%
40%-130%
25%-130%
25%-130%
25%-130%
Ratio
0.75
0.79
1.53
1.50
0.48
1.21
0.43
1.02
0.84
8T Flags
15:35
16:22
20:50
22:17
25:19
26:10
28:18 -
29:13
31:42
70%-140%
70%-140%
70%-140%
70%-140%
70%-140%
QC Limits
40%-130%
40%-130%
1.51
0.49
1.30
0.43
Ratio
0.48
0.49
0.80
1.24
16:23
21:49
25:12
26:05
29:33
RT Flags
26:40
25:55
16:09
26:28
Data Reviewer
11/11/96
Page 2 of2
X237.PSR YIJ4. LARS 6.08.00
Triangle Laboratories, Inc.®
801 Cap'rtola Drive • Durham, North Carolina 27713
Phone: (919) 544-5729 • Fax: (919) 544-5491
Printed: 16:0311/11/96
54
-------
TLI Project:
Client Sample:
39291rl
23A-1
Toxicity Equivalents Report
Analysis File: T966601
Client Project:
Sample Matrix:
TLI ID:
Sample Size:
Dry Weight:
GC Column:
Eastern Ridge Lime Facility
M23TRAIN Date Received: 10/19/96
143-23-lA,B Date Extracted: 10/21/96
Date Analyzed: 10/31/96
1.000 Dilution Factor: n/a
n/a Blank File: T966616
DB-5 Analyst: BB
Spike File:
ICal:
ConCal:
% Moisture:
% Lipid:
% Solids:
SPX23708
TF53286
T966598
n/a
n/a
n/a
2,3,7,8-TCDD
1,2,3,7,8-PeCDD
1,2,3,4,7,8-HxCDD
1,2,3,6,7,8-HxCDD
1,2,3,7,8,9-HxCDD
1,2,3,4,6,7,8-HpCDD
1,2,3,4,6,7,8,9-OCDD
TOTAL PCDD
2,3,7,8-TCDF
1,2,3,7,8-PeCDF
2,3,4,7,8-PeCDF
1,2,3,4,7,8-HxCDF
1,2,3,6,7,8-HxCDF
2,3,4,6,7,8-HxCDF
1,2,3,7,8,9-HxCDF
1,2,3,4,6,7,8-HpCDF
1,2,3,4,7,8,9-HpCDF
1,2,3,4,6,7,8,9-OCDF
TOTAL PCDF
0.01
0.02
0.02
0.02
0.007
0.04
0.09
0.30
0.01
0.01
0.03
0.01
0.01
0.02
0.04
0.02
0.06
x
x
X
X
X
X
X
X
X
X
X
X
X
X
X
X
X
1
0.5
0.1
0.1
0.1
0.01
0.001
0.1
0.05
0.5
0.1
0.1
0.1
0.1
0.01
0.01
0.001
0.01
0.01
0.002
0.002
0.0007
0.0004
0.00009
0.0252
0.03
0.0005
0.005
0.003
0.001
0.001
0.002
0.0004
0.0002
0.00006
0.0432
Total EPA TEFs, 1989a: 0.0684 ng
Page 1 of 1
TEFPR vS.08. LARS 6.08.00
Triangle Laboratories, Inc.®
801 Capitola Drive * Durham, North Carolina 27713
Phone: (919) 544-5729 • Fax: (919) 544-5491
Printed: 16:20 11/11/96
55
-------
Data Review By:
..Date
Calculated Noise Area:
4.50
The Total Area for each peak with an ion abundance ratio outside
ratio limits has been recalculated according to method requirements.
Page No.
11/11/96
Listing of T966601B.dbf
Matched GC Peaks / Ratio / Ret. Time
Compound/
M_Z.... QC.Log Omit Why ..RT. OK Ratio Total.Area... Area.Peak.1.. Area.Peak.2.. Rel.RT Compound.Name.. ID.
TCDF
304-306
DC NL 0
13:
0.
:00 RO
:05
DC SN 13:11 RO
D
M
M
M
304-306
13C12-TCDF
316-318
316-318
TCDD
320-322
D
D
D
M
M
D
320-322
13
13
13
14
14
14
D cb 14
15
15
15
15
16
16
:25 RO
:35
:S1
:04
:24
:39
:53
:00
:11
:24
:37
:03
:18
65-0.89
1.
0,
0,
0
0,
0.
0.
0
0
o.
0
0
0
0
0
0
13 Peaks
DC NL 0
14
15
15
16
0.
:00 RO
:38
:10
:35
:03
.16
.75
.54
.98
.71
.81
.84
.83
.69
.73
.80
.85
.82
.77
.68
.77
1
6
91
1
60
54
227
160
126
122
98
159
48
40
145
28
22
,289
.55
.48
.75
.27
.31
.59
.90
.98
.02
.53
.90
.60
.50
.48
.61
.79
.43
39.
33.
22.
102.
73.
57.
49.
71.
22.
18.
63.
11.
9.
09
30
48
18
57
65
79
20
40
20
31
54
95
52
34
31
125
87
69
72
88
26
22
82
17
12
65-0.89
0
0
0
0
0
4 Peaks
DC NL 0
14
14
D SN 14
15
DC SN 15
D SN 15
D SN 15
16
16
D SN 16
DC SN 16
DC SN 17
0.
;00 RO
:02
:20
:32
:08
:30 RO
s34 RO
:48
:08 RO
:16 RO
:23 RO
:34 RO
:37
.97
.86
.74
.75 9
.73
9
4
59
30
,097
88
,276
m**!!-!
.26
.68
.61
.71
.44
.44
is* / rrv*
.65-0.89
1
0
0
0
0
0
2
0
0
0
0
1
0
.56
.80
.70
.88
.69
.91
.72
.71
.93
.95
.61
.40
.83
5 Peaks
2
94
38
5
39
1
2
6
14
15
9
2
2
202
,71
.87
.04
.31
.41
.70
.64
.98
.27
.81
.01
.05
.14
.40
27.
13.
3,896.
37.
52
02
37
44
32
17
5,201
51
0.
.39
.05
.83
.41
.33
.33
.23
.70
.20
.30
.17
.07
.84
0.
.16
.59
.34
.00
828-1.138
0.000
0.840
0.846
0.861
0.872
0.889
0.903
0.924
0.940
0.955
0.963
0.974
0.988
1.002 2378-TCDF AN
1.030
1.046
936-1.064
0.000
0.939
0.973
1.000 13C12-2378-TCDF ISO
1.030
42.
15,
16.
18
71
09
7.49
8.44
52
22
23
8
8
0.
.69
.33
.32
.06
.93
846-1.086
0.000
0.857
0.876
0.888
0.925
0.947
0.951
0.965
0.986
0.994
1.001 2378-TCDD AN
1.012
1.076
Triangle Laboratories, Inc.® Analytical Services Division
801 Captela Drive • Durham, North Carolina 27713
Phone: (919) 544-5729 • Fax: (919) 544-5491
Printed: 15:51 11/11/96
56
-------
Page No.
11/11/96
Listing of T966601B.dbf
Matched GC Peaks / Ratio / Ret. Time
Compound/
M_Z..., QC.Log Omit Why ..RT. OK Ratio Total.Area... Area.Peak.1,. Area.Peak.2.. Rel.RT Compound.Name.. ID..
37C1-TCDD
328
328
13C12-TCDD
332-334
332-334
PeCDF
340-342
D
D
D
D
D
340-342
13C12 -PeCDF
352-354
352-354
PeCDD
356-358
DC NL 0 : 00
DC WL 14 : 12
DC WL 14:17
14:58
16:23
2 Peaks
DC NL 0:00
15:09
16:09
16:22
16:46
4 Peaks
DC NL 0:00
17:59
DC SN 18:56
19:28
19:39
D SN 19 : 54
D SN 20:14
20:27
D SN 20:45
20:52
D SN 21:04
21:50
D SN 22:01
DC SN 23:03
6 Peaks
DC NL 0 : 00
19:38
20:23
20:50
21:13
21:49
5 Peaks
DC NL 0:00
19:54
DC SN 20:02
DC SN 20:05
DC SN 20:14
0,
RO
RO
1.
RO
RO
RO
RO
RO
RO
RO
1.
RO
RO
3,
4,
65-0.89
3.59
0.81
0.
0.
0,
80 4,
79 7,
97
12,
32-1.78
0.
1.
0.
1.
1.
2.
0.
1.
1.
1.
1.
1.
5.
1.
71
41
36
56
52
23
87
57
66
63
25
74
31
13
0.92
2.16
4.22
387.00
836.40
223.40
2.82
34.46
228.68
855.40
89.95
208.49
2.65
71.89
0.92
20.23
94.76
13.46
2.58
44.03
11.34
15.69
11,55
16.26
3.98
0.58
262.86
387.
3,836.
15.
1,885,
3,474,
49,
.00
,40
.43
.31
.37
.38
0.878-1.122
0.000
0.868
0.873
0.914
1.001 37C1-TCDD
0.878-1.122
0.000
19.03 0.926
2,343.37
4,381.03
50.73
0
1
1
.987 13C12-1234-TCDD
.000 13C12-2378-TCDD
.024
SUR1
RSI
IS1
42
12
57
26
9
10
.11
.32
.12
.93
.73
.32
.32-1.78
0.74
1.
63
1.07
1.53 8,
RO
1.83
1.51 4,
1
RO
RO
RO
RO
13,
.32-1.78
1.04
1
0
1
0
.08
.25
.62
.19
1.15
21.20
12.36
480.20
20.61
569.62
103.99
ia/T\I? t
revoke /
1.97
38.05
0.56
1.23
1.45
13
7
5,134
14
2,748
.15
.52
.53
.79
.94
0.855-1.112
29.78
7.91
37.64
17.10
5.96
5.94
0.
8.05
7.01
3,345.67
8,08
n, 820. 68
0
0
0
0
0
0
0
0
0
1
1
1
1
1
808
0
0
0
1
1
1
.000
.863
.909
.934
.943
.955
.971
.982
.996
.002 12378-PeCDF
.011
.048 23478-PeCDF
.057
.106
-1.192
.000
.942
.978
.000 13C12 -PeCDF 123
.018
.047 13C12-PSCDF 234
AH
KS
IS2
SUR2
PeCDD Follows —
23
.13 •
0.
21.44
885-1.034
0
0
0
0
0
.000
.893
.899
.901
.908
Triangle Laboratories, Inc.® Analytical Services Division
801 Capitola Drive * Durham, North Carolina 27713
Phone: (919) 544-5729 • Fax: (919) 544-5491
Printed: 15:51 11/11/96
(
-------
Page No.
11/11/96
Listing of T966601B,dbf
Matched GC Peaks / Ratio / Ret. Time
Compound/
M_2.... QC.Log Omit Why ,.RT. OK Ratio Total.Area... Area.Peak.1.. Area.Peak.2.. Rel.RT Compound.Name.. ID.
D
M
D
D
D
356-358
13C12-PeCDD
368-370
368-370
HxCDF
374-376
M
M
374-376
13C12 -HXCDF
384-386
384-386
D
DC
D
DC
DC
D
D
DC
DC
DC
DC
DC
DC
DC
DC
DC
DC
DC
DC
DC
DC
DC
DC
DC
DC
SN
SN
SN
SN
SN
SN
SN
SN
SN
SN
SN
SN
SN
WH
WH
WH
3
NL
SN
3
NL
SN
SN
SN
SN
SN
5
NL
5
20:34
20:36
20:56
21:07
21:20
21:30
21:33
21:39
21:55
22:04
22:08
22:18
22:23
22:28
22:42
23:07
23:10
23:16
Peaks
0:00
20:52
22:17
22:28
22:57
Peaks
0:00
24:05
24:16
24:36
24:48
25:13
25:20
25:40
25:44
25:55
26:54
Peaks
0:00
24:04
25:12
25:19
25:55
26:40
Peaks
RO
RO
RO
RO
RO
RO
RO
RO
RO
RO
RO
RO
RO
RO
RO
1.
RO
RO
RO
1.
RO
RO
RO
RO
RO
0
RO
RO
0.
1.
1.
1.
1.
2.
0.
2.
0.
1.
1.
0.
1.
4.
2.
3.
0.
2.
92
90
92
89
50
18
93
27
86
77
60
28
28
76
37
24
84
40
2.
0.
25.
4.
18.
1.
1.
3.
6.
2.
2.
1.
1.
2.
2.
1.
0.
1.
82.
45
74
76 19.40
08
98 11.39
25
76
34
89
55
81
86
45
01
01
05
53
35
79
3-2-1.78
19.
1.
1.
1.
0.
13
29
50
56
63
,05-1.43
0.
1.
1.
5.
0.
1.
1.
6.
6.
1.
.1.
96
19
17
00
68
34
40
69
00
23
21
0.
3,
4,532.
421.
1.
20
48 2.12
46 2,720.57
27 256.93
06
0
0
10.10 0
0
7.59 0
0
0
0
0
0
0
1
1
1
1
1
1
1
.923
.924
.939
.948
.957
.965
.967
.972
.984
.990
.993
.001 12378-PeCDD
.004
.008
.019
.037
.040
.044
AN
0.821-1.179
0
1.64 0
1,811.89 1
164.34 1
1
.000
.936
.000 13C12-PeCDD 123
.008
.030
IS3
4,957.21
i PsCDD / HxCDF Fol lows ~ —
3.
13.
26.
0.
1.
21.
10.
0.
0.
9,
1.
81.
13
64 7.40
33 14.17
58
.37
07 12.07
.54 6.15
.36
.36
.63 5.31
,15
,21
.43-0.59
0.63
0.38
0.49
0.48
0.49
0.48
4.06
12.21 4.14
3,115.15 1,018.37
5,922.90 1,928.88
3,446.08 1,127.73
2,801.66 909.01
15,298
.00
0.945-1.064
0
6.24 0
12.16 0
0
0
9.00 0
4.39 1
1
1
4.32 1
1
.000
.951
.959
.972
.980
.996 123478-HxCDF
,001 123678-HxCDF
.014
.016
.024 234678-HXCDF
.063
AN
AN
AN
0.842-1.158
0
10.84 0
2,096.78 0
3,994.02 1
2,318.35 1
1,892.65 1
.000
.951
.995 13C12-HXCDF 478
.000 13C12 -HxCDF 678
.024 13C12-HXCDF 234
.053 13C12-HXCDF 789
STO3
IS4
ALT2
ALT1
Triangle Laboratories, Inc.® Analytical Services Division
801 Captela Drive * Durham, North Carolina 27713
Phone: (919) 544-5729 • Fax: (919) 544-5491
Printed: 15:51 11/11/96
53
-------
Page No.
11/11/96
Listing of T966601B.dbf
Matched GC Peaks / Ratio / Ret. Time
Compound/
M_Z.... OC.Log omit Why ..RT. OK Ratio Total.Area... Area.Peak,1.. Area.Peak.2.. Rel.RT Compound.Nam*.. ID..
HXCDD
390-392
D
H
390-392
13C12-HXCDD
402-404
402-404
HpCDF
408-410
M
408-410
13C12 -HpCDF
418-420
418-420
DC
D
DC
DC
DC
DC
DC
DC
DC
DC
DC
DC
DC
DC
DC
DC
DC
DC
DC
DC
DC
NL
SN
SN
SN
SN
SN
SN
SN
SN
SN
SN
3
NL
4
NL
SN
SN
SN
SN
SN
SN
SN
3
NL
2
0:00
24:44
24:51
25:04
25:15
25:24
25:31
25:42
25:45
25:55
26:11
26:20
26:23
26:27
Peaks
0:00
25:30
26:05
26:10
26:28
Peaks
0:00
28:18
28:33
28:40
28:54
28:58
29:04
29:10
29:15
29:20
29:34
Peaks
0:00
28:18
29:33
Peaks
1.
RO
RO
RO
RO
RO
RO
RO
RO
RO
RO
1.
RO
0.
RO
RO
RO
RO
RO
0.
RO
rtjjuve
05-1.43
0.85
2.62
0.23
1.42
1.28
0.48
1.37
1.20
1.63
6.48
0,52
0.21
0.65
1.95
05-1.43
1.10
0.90
1.30
1.21
1.24
88-1.20
0.98
0.89
1.19
1.05
1.68
0.47
1.02
3.76
1.05
3.18
1.44
,37-0.51
0.63
0.43
0.43
. njci_jjj« / HKUJJU roxxows •
0.939-1.017
2.
2.
0.
0.
118.
0.
9.
0.
0.
0.
1.
0.
0.
5.
132.
19
91
20
75
00 66.27
43
64 5.57
99
43
52
90
56
58
00 4.35
64
51.73
4.07
2.23
0.
0.
0.
0.
0.
0.
0.
0.
0.
0.
1.
1.
1.
1.
000
945
950
958
965
971
975
982
984
990
001 123678-HxCDD
006
008
Oil 123789-HxCDD
AN
AN
0.962-1.038
3.
8.
2,463.
5,271.
2,751.
10,494.
2.
37.
85
00 4.44
53 1,392.56
44 2,886.13
60 1,520.98
57
34
31 17.60
5.38 2.92
10.00 5.12
4.91
1,070.97
2,385.31
1,230.62
0.
0.
0.
0.
1.
1.
000
975
997 13C12-HXCDD 478
000 13C12-HXCDD 678
Oil 13C12-HXCDD 789
SUR4
IS5
RS2
995-1.051
0.000
19.71
2.46
4.88
0.69
1.08
1.66
0.92
1.72
0.69
2.49
52.
5
4,555
1,884
.69
.08
.47 1,366.52
.64 562.98
0.
3,188.95
1,321.66
1.000 1234678-HpCDF
AN
1.009
1.013
1.021
1.024
1.027
1.031
1.034
1.037
1.045 1234789-HpCDF
AN
929-1.141
0
.000
1.000 13C12-HpCDF 678
1
.044 13C12-HpCDF 789
IS6
SUR5
6,440.11
AYuwa* HrvTTH? / UnTTsn VrtTl mia
Triangle Laboratories, Inc.® Analytical Services Division
801 Capitola Drive • Durham, North Carolina 27713
Phone: (919) 544-5729 • Fax: (919) 544-5491
Printed: 15:51 11/11^96
-------
Page No.
11/11/96
Listing of T966601B.dbf
Matched GC Peaks / Ratio / Ret. Time
Compound./
M_Z. — QC. Log Omit Why
HpCDD
424-426
,-RT. OK Ratio Total.Area... Area.Peak.1.. Area.Peak.2. . Rel.RT Compound.Name.. ID.
424-426
13C12-HpCDD
436-438
436-438
DC
DC
DC
DC
DC
DC
DC
DC
DC
NL
WL
SN
SN
SN
WH
WH
2
NL
SN
2
0:
28;
28:
28;
28;
29;
29;
29:
29:
:00
;24
:29
:36
:56
:08
:14
:25
:32
0.
RO
RO
RO
RO
RO
RO
.88-1.20
2
0
0
0
2
1
0
2
2
.19
.85
.35
.94
.80
.15
.91
.14
.83
Peaks
0;
29:
29:
29:
;00
t!3
:27
:38
0,
RO
RO
RO
,88-1.20
1
1
0
0
.50
.02
.78
.82
Peaks
IK
1.27
1.00
0,41
18.57
0.92
0.56
18.39
0.75
1.43
36.96
8.99
5.75
0.973-1.006
0.000
0.972
0.975
9.58 0.979
0.990
0.997
9.64 1.001 1234678-HpCDD
1.007
1.011
AN
1.50
1.02
0.78
0.82
4.10
4,337.78
4.17
1.98
4,341.95
2,192.09
2.13
2,145.69
2.72
0.966-1.034
0.000
1.000 13C12-HpCDD 678 IS7
1.008
1.014
Above: HpCDD / Octa-CDD and CDF Follows
OCDF
442-444
442-444
0.76-1.02
DC NL 0:00 0.86 3.53
31:46 0.82 28.60
1 Peak 28.60
12.85
0.874-1.126
0.000
15.75 1.002 OCDF
AN
OCDD
458-460
458-460
0.76-1.02
DC NL 0:00 RO 0.61
31:42 0.96
DC SN 32:06 RO 1.09
1 Peak
0.92
41.14
1.42
41.14
20.16
0.874-1.126
0.000
20.98 1.000 OCDD
1.013
AN
13C12-OCDD
470-472
470-472
DC
NL 0:00
31:42
1 Peak
0.76-1.02
1.02
0.84
0.89
6,836.33
6,836.33
3,118.27
0.995-1.006
0.000
3,718.06 1.000 13C12-OCDD
IS8
Column Description "Why" Code Description QC Log Desc.
M_Z -Nominal Ion Mass(es)
,.RT. -Retention Time (miuss)
Rat.l -Ratio of M/H+2 Ions
OK -RO=Ratio Outside Limits
Rel.RT-Relative Retention Time
*** End of Report ***
WL-Below Retention Time Window
WH-Above Retention Time Window
SN-Below Signal to Noise Level
-------
File:T966601 #1-835 Acq:31-OCT-199"B 22:27:16 EH- Voltage SIR 70T~
319.8965 F:2 Exp:EPCUS
Sample Text:23A-l TLI#39291R1
100% 15;08
50:
INJ. TIME = 22:30 File Text:23A-l TLI#39»
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15iOO 16:00 17iOO 18:00 Time
File:T966601 #1-835 Acq:31-OCT-1996 22:27:16 EI+ Voltage SIR 70T
321.8936 F:2 Exp:EPCUS
Sample Text:23A-l TLI#39291R1 INJ. TIME = 22:30 File Text:23A-l TLI#39»
100% 15;08 _4.5E4
50:
18:00
Time
16:00 17:00
File:T966601 #1-835 Acq:31-OCT-1996 22:27:16 EI+ Voltage SIR 70T
331.9368 F:2 Exp:EPCUS
Sample Text:23A-l TLI#39291R1 INJ. TIME = 22:30 File Text:23A-l TLI#39»
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50:
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16:09
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15:00 16:00 17:00 18:00 Time
File:T966601 #1-835 Aeg:31~OCT-1996 22:27:16 EI+ Voltage SIR 70T
333.9338 F:2 Exp:EPCUS
Sample Text:23A-l TLI#3929lRl INJ. TIME = 22:30 File Text:23A-l TLI#39»
100% 16; 22 _1.0E7
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16:08
15:00
16:00
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-------
File:T966601 #1-835 Acqi31-OCT-lS96 22:27:16 EI+ Voltage SIR 70T Soisei2150
303.9016 Fs2 BSUB(2S6, 30, -3. 0) PKD(5, 3,1, 0 . 10%, 8600 . 0, 0. 00%, F,F) EjcpsEPCOS
TRIANGLE LRBS Text:23A-l TLI#39291R1
1004
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305,8987 F:2 BSUS(256, 30, -3. 0) PKD(5, 3,1, 0.10%, 7392. 0, 0. 00*,F,F) EXftEfCOS
TRIANGLE LABS Text:23A-l TLH39291R1
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sol
601
401
201
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' 16iOo'
2.8E5
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File:T966601 #1-835 Acq:31-OCT-1996 22:27:16 EI+ Voltage SIR 70T Noise:1164
315.9419 F:2 SSUB( 256, 30, -J. 0) tXD(5,3,l, 0. 101,4656. 0,0.00%,jr, F) Eip:EPCUS
TRIANGLE LASS Text:23A-l TLIt39291Rl
1003
aol
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401_
201
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13:00 14:00 15:00
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' 17:00' ' ' ' ' 18sOQ Time
File:T966601 #1-835 Acq:31-OCT-1996 22:27:16 EI+ Voltage SIR 70T Jfoi.se:1204
317.9389 F:2 BSUB(256, 30, -3 . 0 ) PKD( 5, 3,1, 0 . 10%,4816. 0, 0. 00*,F,F) Exp:EPCUS
TRIANGLE LASS Teit:23A-l TLH39291R1
1003
sol
601
40J
201
0:
AS.
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is'soo' ' ' ' 14: 00 isioo'
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20E7
I
'is.'oo
-1 . 3E7
,1.0E7
.7.8E6
15.2E6
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O.OEO
' 17'sOo' ' ' ' 18:00 Time
File:T966601 #1-835 Acq:31-QCT-1996 22:27:16 EI+ Voltage SIR 70T
330.9792 F:2 Exp:EPCUS
TRIANGLE LABS Text:23A-l TLH39291R1
100$
sol
eol
402
201
o:
i^H^^-^^-^UiSJjiii^^
13 too' ' ' ' ' 14*00 ' ' 15s 00
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17:31 17:56r4-1E7
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' 17:00' ' ' ' IStOO Time
File:T966601 #1-835 Acq:31-OCT-1996 22:27:16 EI+ Voltage SIR 70T
375.8364 F:2 Exp:EPCt!S
TRIANGLE LABS Text:23A-l TLH39291R1
100J
sol
eol
4ol
201
o-
13 -19 13:58
1 1 i 1 15s 1.9
I j I 14:24 <**•** 1 i
it HI 1 it n 1
i fill 13 f 40 ll 1 § 1 ml n J
j I 1 111 1 111 1 j ll 1 I I I 15 • H-2 N
I Jiljl fll nlli A m -jA 1 nil IL An J \ n& 1 IJII In 1 n JU
UIWu^yVL/u'tW wL>*Ji V«A/*^V/ i IA*/W**W lAjVWW HuLAAJVl \*»A/ lAW^—
13:00 14:00 ' ' IS: 00
IJKT. TIKE " 22:30
16
15 1 45
1 16.-15
* A 1 1 A »
m In iJ « A
•Arl MlMlmli
tv\J IL/w11 ifwUif"wl wviU
16-00
45 1.2E4
17:49
11 17f°7 1 1 (1 1
U 1 11 1
1 1 iu 1 I Ml
IklJnMlJlM nlk
U» UUlfV U LAlll/VVviLJU "rv/
-9.4E3
'-.7.1E3
'•.4.7E3
-.2.4E3
• 0 . OEO
17-00 IflsOO Time
-------
FilesT966601 #1-835 Acq:31-OCT-1996 22:27sl6 SI* Voltage SIS 70T JWaiserllSl
319.8965 F:2 BSUS(2S6,30, -3. 0) PKD(S,3, 1,0 .101,4764 .0,0. 00*,F,F) ExpsEPCUS
TSIANSLE LASS TeXts23A-l TLI#39291M1 £KT. TIKE - 22:30
1001
80:
so:
401
201
R4.22E5
A
A1.57E5
A Al . 61ES
\ I \ r\ A1.11S4 A6.67E4
14-00 ' ' ' ' 15:00 ISsOO ' 17s 00 ' ' ' ' 18s OC
-1.1E5
Ls.OE4
'-S.BE4
'-4.SE4
L2.3E4
LO.OEO
Time
file:T966601 #1-B35 Acise:757
333.9338 Ft2 BSUS(256, 30, -3 .0) PKD(5, 3,1, 0.10%, 3188 . 0, 0. 00%, FrF) Exp:EPCUS
TRIANGLE LABS Texts23A-l TLI #39291X1 HKT. TIKE - 22:30
1003,
soj
so:
40:
20:
o-
A4.
A2.34E7
A
Al
38E7
I
141-00 15:00 16-00 17:00 18.-0(
1 . OE7
-8.0E6
'-6.0E6
"•.4.0E6
L2.0ES
" 0 . OJTO
! Time
File:T966601 #1-835 Acq:31-OCT-1996 22:27:16 EH- Voltage SIS 70T Noiae:461
327.8847 F:2 BSUB(256r30, -3 .0) PKD(5,3,l,0.10\,1844.0rO.OO\,FrF) ExpiEPCDS
TRIANGLE LABS Text:23A-l TLI#39291X1 IJKT. TIME = 22:30
1003
80.
60.
40.
20.
0
A3.
A3.87E6
y\ /
84E7
{
14100 ' ' ISsOO ' ' ' 1S100 ••'•'• 17't00 ' 18:01
8.SES
-7.1ES
-5.4E6
13 . 6E6
.1 . 8E6
'• O.OEO
3 Tim*
FileiT966601 #1-835 Acqs31-OCT-1996 22:27:16 EI+ Voltage SIS 70T
330.9792 F:2 Exp-.EPCUS
TRIANGLE LABS Text.t23A.-l TLH39291S1 isy. TIME = 22:30
1003
80.
60.
40.
20.
0
^_ 14:12 JLdjJJ 15:18 Iffll* 16:33 17:31 17:56
^-~-- ^'^-••v^/»*v%^^*-w^/\*.**"^ Vr^^^^^^*%r-\^^^*^ J-Lj*^*f^s^~~*'~l *sx^*^— - *~^ ^— " — - ~ - ^w^— ^— * -^ —*•**-«-*
— -~~ - ~ — ^r-x^^*— j ' **~ »
14.-00 15:00 15-00 17.-00 18-0(
,_4 . OE7
.
-.3.2E7
•-2.4E7
11.6E7
18.0E6
"' O.OEO
3 Time
83
-------
File:T966601 #1-835 Acq:31-OCT-199S 22s27il6 EI+ Voltage SIX 70T NOise:S03
33S.8597 F:2 BSUB(256,30, -3.0) PJO>(5,3,1, 0.10%,3212. 0, 0. 00%,F,J*; Sxp:EFCUS
TRIANGLE LABS Tezts23A~l TLH39291S1 IJKT. TIME =• 22t30
100* A5.71E5
18:00 19:00 20tOO 21:00 22'iOO
FilesT96S601 #1-835 Acq:31-OCT-1996 22s27il6 EI+ Voltage SIR 7QT Koiae:1140
341.8567 F:2 3SOB(256,30,-3.0} PXD(5,3,1,0.101,4560.0,0.00\,f,Jf) ExpiEPCUS
TRIANGLE LABS Tert.-23.fl-I TLH39291R1 XMT. TIME - 22:30
1004 A3.J6ES
18s00 19:00 20:00 21:00 22:00
File:T9666Ql #1-835 Acq:31-OCT-1996 22:27:16 EI+ Voltage SIR 701 Noise:351
351.9000 Fi2 SSCB(2SS,30r-3.0) PXD(Sr3rl,0.10*,1404 ,0,0.00%,F,F) Ezp:EPCUS
TRIANGLE LABS Teit:23A-l TLH39291S1 JJKT. TIME - 22:30
A5.13E7
40:
201
OJ
A2. 75E7
18:00 19100 20:00 21:00 22:00
File:T96SB01 #1-835 Acqi31-OCT-J.996 22:27:16 EI+ Voltage SIR 70T Noises477
353.8970 F:2 BSUB(256, 30, -3 . 0) PKD(5, 3,1, 0 .10%,1P08. 0,0 . 00%,F,F; Exp:EPCUS
TRIANGLE LABS Teits23A-l TLI#39291S1 IlKT. TIME « 22:30
100* A3.35E7
ao:
60:
401
201
0:
Al.82E7
18:00 19:00 20:00 21:00 22:00
FilsiT966601 #1-835 Acq:31-OCT-1996 22:27:16 E1+ Voltage SIR 70T
330.9792 Fs2 Exp:EPCUS
TRIANGLE LABS Text:23A-l TLI&39291R1 INJ. TIME = 22:30
80d
sol
40:
20:
0,
18.-00 19sOO 20:00 21:00 22:00
FilesT966601 #1-835 Acq:31-OCT-1996 22:27:16 EI+ Voltage SIR 70T
409.7974 Fs2 Exp:EPCUS
TRIANGLE LABS Text:23A-l TLI#39291S1 1MJ. TIME = 22:30
1001
80:
60:
40:
20:
o.
IB
03
21:19
IB- 00
22:21
19sOo
19:17 13.33 I I 20:49 | i I
Oo' 20:00 '21-00
31,-55
23:00
23100
23:00
23:00
.6.5E4
.5.2E4
3. 9E4
2.6E4
1.3E4
.O.OEO
Time
.1. 2E7
.9.4E6
.7.1E6
.4.726
.2.4E6
. 0. OEO
Time
.7.7E6
.6.2E6
.4.6E6
.3. 1E6
.1. 5E6
.O.OEO
Time
.4.0E7
.3.2E7
.2.4E7
.1.6E7
.7.9E6
.O.OEO
Tine
22:00
.1. 7E4
.1.3E4
.1. OE4
.6.7E3
.3.4E3
.O.OEO
Time
B4
-------
F3.1e:T9666OJ. #1-835 &cq: 31-OCT-1996 22:27:16 SI+ Voltage SIS 7QT OoiBSi602
355.3546 F:2 SSUS(256,30,-3 .0) PKD( 5, 3,1, 0. 10%, 2408. 0,0. 00%, F, T) EzptEPCUS
TRIANGLE TABS Text: 23A-1 TLI#39291Sl IKT. TIME ** 22:30
1001
'.
801
601
401
201
g'
A2 . OE5
A2.31E5
I I" A1.14E5
In
II A4.19E4
1 M >m 7<:«.3 A1.49E4 \ 11 A at
I 1 A8.76E3 i H \ I L A2.97S4 f\
jL~$&SLk^^
20:00 ' ' ' ' 21:00 ' " 22:00
-5 . OE4
12m A2.03E4
AA3.76S4 1 " ••'••'-'4
(!"-* * ' w**^ B |
-4.0E4
.3 . OE4
.2.QE4
.1 . OE4
" 0 . OKI)
23:00 Tine
File.-WSSSOl #1-835 Acq:31-OCT-1996 22.-27.-1S EI+ Voltage SIS 70T Ndiae:577
357.8516 Fs2 BSUB(256,30, -3.0) PKD(5,3,1, 0.101,2308.0,0. 00\,F,F) Eip-.EPCUS
TSIAKGZE LASS Texti23A-l TLI#39291S1 IKT. TIME = 22:30
1004
so:
so:
"
401
20.
0"
1
(
1 1. A9 . 65E4
\ Jj A7.59E4
A I A4 . 85E4
d 1
n n M .
/ !\l\
04E4
^A8.86E3
1 A4.11E3
,4.2E4
13 . 4E4
-2.5E4
11 . 7E4
18.4E3
~ n . oiro
20:00 .... ai\}00 ' 22:00 ' 23:00 ' ' Time
FilesT966601 #1-835 Acq:31-OCT-1996 22:27:16 EI+ Voltage SIS 70T Noises 764
367.8949 Fs2 BSVB(256,30,-3 .0) PXD(5,3,1, 0.101,3056, 0,0,00%,F,F) ExpsEPCOS
TRIANGLE LASS Text.-23.fl-l 3X1 #35291X1 JWJ. TIME = 22:30
100*
so:
so:
401
201
•
0.
A2.
J
20:00 21 .-00 22:00
72E7
|
1
A2.57ES
V/V
-.S.9ES
15.5FS
1«.1E«
12.8ZS
11 . 4E6
" 0 . OEO
23 : 00 Time
File:T966601 #1-835 Acqi31-OCT-1996 22:27:16 EI+ Voltage SIS 70T Noiae:40
369.8919 F:2 BSUB(256,30,-3.0) PKD(5, 3,1,0. 10*,16Q .0,0. 00\,F,F) Exp:EPCUS
TRIANGLE LASS Texts 23A-1 TLI#39291K1 IKT. TIME = 22:30
1003
so:
so.
40.
201
0
Al.
/
20:00 ' ' ' 21:00 22:00
FiZe:TSSS601 #1-835 Acq:31~OCT-1996 22:27:16 EI+ Voltage SIS 70T
330.9792 Fs2 ExpiEPCUS
81E7
Al . 64ITS
XA
-4.5E6
13 . 6E6
12 . 7E6
11 , 8E6
'.9.1E5
" 0 . OEO
23 : 00 riffle
TRIANGLE LASS Tejct:23A-l TLI#39291M1 IlKr. TIME " 22:30
1003
80.
SO.
40.
20.
0.
^_>ji24j£^^kr45^£-, 20i52 21:32 21:51 22s04
20:00 21:00 " ' ' ^ 22:00
2J.-02 _*-OE7
2j_1922:32 ^~-^~~--^
•
'.3.2E7
'.2.4E7
11 . 6E7
'.7.9E6
" O.OEO
23 1 00 Time
-------
FilesT9666'01 #1-504 Ac±se:863
373.B208 F:3 BSUB(256, 30,-3 .0) PKD(5,3,1, 0.10%, 3452. 0,0. 00%, f,F) Exp:EPCUS
TXIANSZE LABS Text:23A-l TLI#39291K1 HKT. TIME - 22:30
2
-------
KISTJWffWOM 11 -5W Aoq,31-OCT-159S " 22:27:16 E*+
Voltage StS 76t &oime:6Q7
389.8156 F:3 BSUS(256,30, -3. 0) PKS( 5, 3,1, 0.10%,2428. 0, 0. 00%,F,F; ExpsEPCUS
TRIANGLE LABS Text:23A-l TLH39291R1
100J
so:
eo:
40:
20:
A6.63JE5
1
A3.41JT4 / V M.37X4
« ***** » i< ^^ r\. - ^^
24:36 " 24:48 25:00 25:12 25*24 25:36
File:T966601 #1-504 Acqs31-OCT-1996 22:27:16 EH-
JKT. TIKE = 22:30
Al . 491:4
.2.2E5
.1 . 7Z5
.1 . 3Z5
-8.7S4
-4.4E4
O.OEO
25:48 26:00 26*12 26:24 261-36 26.-4S Time
Voltage SIX 70T Kbise:711
391.8127 F:3 BSU3(256,30,-3.0) PJO>(5,3,1, 0,10%,2S44. 0,0, 00\,r,F) ExpsEPCUS
TRIANGLE LABS Text:23A-l TLI#39291S1
1003
so:
eo:
40:
20:
0"
A5.17E5
A
ft
A1^36E4 J \^ Aj^E^4
24* iff ' 24:48 ' '25:00 ' 25*12 ' '25:24 ' 25:36
File, "1966601 #1-504 Acq:31-OCT-1996 22:27:16 EI+
I1W. TIME = 22:30
A2.02E4 A2.23E4
-1 . 6E5
_1 . 3E5
-9.5E4
-.6.3E4
-3.2E4
" 0_ OFO
25:48 ' '26:00 26:12 ' 26:24 ' 26:36 ' '26:48 ' Time
Voltage SIS 70T Sbiae:1011
401.8558 F:3 BSUS(256,30,-3.0) PKDf5,3,l,0.10%,4044.0,0.00%,I-,F> Exp-.EPCUS
TRIANGLE LABS Text:23A-l TLI#39291R1
100S
so:
eo:
40.
201
0"
24 Jiff ' 24:48 ' 25: 00 ' "25 1 12 ' '25:24 ' '25136 '
file : T966601 #1-504 Acq:31-OCT-1996 22:27:16 EI+
ISJ, TIME = 22:30
A2.89E7
h
ft
I A1.S2E7
\ h
A A
v A
J l V. / V
_9 . 5S6
'.7.6E6
15 . 7E6
13.8E6
11 . 9E6
' 0 . OSO
'25:48 ' '2'ffsOO ' '26s 12 ' ' 26\24 ' '261 36 ' '26\48 ' ' Time
Voltage SIS 70T Noiae:914
403,8529 T:3 BSUB( 256,30, -3. 0) PKD( 5, 3,1, 0.101,3656. 0, 0. 00%,F, T) Exp:EPCVS
TRIANGLE LABS Text:23A~l TLX#39291X1
1001
80_
60_
40.
20.
0.
24 Jiff 24:48 25*00 25:12 ' 25s 24 ' 25 Jiff
JJRT. TIME = 22:30
A2.39E7
A
1 A1.23E7
t ! >|
A A
V A
/ i V i V
7.9E6
'.6.3E6
.4 . 7E6
13 . irff
11 . 6E6
' o . oiro
25:48 ' '26:00 ' 2ffJl2 26J24' ' 2ffJiff' ' '2ffi48 ' ' Time
File sT9 6 66 01 #1-504 Acq : 31 -OCT-1996 22:27:16 SI+ Voltage SIS 702"
392.9760 F:3 Ezp:EPCUS
TXIA8GLE LASS Text:23A-l TLH39291K1
100.
80.
60.
40.
20.
0.
t, 24:45 25:07 25:27
vArvvyvw — v^\xvvA>«-^s^^^^y^'i^SAj>/~v^A^Ar^s^'
24:3S 24:48 25:00 25:12 25:24 25:36
ISJ. TIME " 22:30
Nr-v^5^x6Jr£3^.^-nA^^ 26-50
r2,0!T7
Ii.6r7
.1.2F7
.8.0E6
_4 . 01T6
O.OEO
25:48 26:00 26.' 12 25:24 26:36 26:48 Tine
B7
-------
File.-T966S01 #1-443 Acq:31-OCT-1996 22:27:16 £1+ Voltage SIS 70T Noiae:579
407.7818 T:4 BSWB(256,30,-3.0) PKD(S,3,1, 0.10%,231S. 0,0 , 00*,F,F) Exp:EPCUS
TXIANSLE LABS Text:23A-l TLI039291S1 XWT. HUE = 22:30
1003,
Al, 76ES
28:12 28:24 28:36 28:48 29'sOO 29:12 29:24 29:36
F±le:T966601 tl-443 Acq:31-OCT-1996 22:27:16 Eli- Voltage SIS 7OT Noise:588
409.7769 F:4 BSOB(256,30, -3.0) PJCD(5,3,l,0.10%,2352.0,0.00*rF,F) EjcpiEPCUS
TRIANGLE LABS Texts23A-1 TLI#39291X1 I3KT. TIME = 22:30
100* A1.97E5
28:12 28:24 28:36 28:48 29'sOO 29:12 29';24 29:36
File:T966601 41-443 Acq:31-OCT-1996 22:27:16 EI+ Voltage SIS 70T No±se:1114
417.8253 F:4 BSUB(256,30, -3. 0) PKD(5,3,l,0.10%t4456,OrQ.001,F,F) ElpiEfCUS
TRIANGLE LABS Teit:23A-l TLI#3S291S1 INJ. TIME - 22:30
100* A1.37E7
801
601
401 I \ A5.63ES
201
Al.69E4
Al.76E4
9.7S4
.7.7S4
L5. 8E4
-3.9E4
.1. 9E4
29:48
30:00
Al.22E4
A9. 79E3
-7.3E4
'•.5.9E4
L4.4E4
'•.2.9E4
-1. SE4
29:48
30:00
.O.OEO
Tine
4.8E6
13. 8E6
'-.2.9E6
-.1. SE6
'-9.5E5
.10. O.EO
28:12 28:24 28:36 28s48 29:00 29:12 29:24 29:36
T±le:T966601 #1-443 Acq:31-OCT-1996 22:27:16 EI+ Voltage SIR 70T Koiae:1762
419.8220 ft 4 BSUB(256,3Q,-3.0) PKD(5, 3,1, 0 .10%, 7048. 0, 0. 001,F,F) Exp:EPCUS
TRIANGLE ZABS Text:23A-l TLI#39291X1 IWT. TIMS = 22s 30
29:48
30:00
100%
so
401
201
A3.J.9E7
A1.32E7
1. 1E7
";S.SE6
.6.6E6
-4.4E6
"-2.2E6
28.-12 28:24 28:36 28:48 29:00 29:12 29:24 29:36
FileiT96S601 #1-443 Acq;31-OCT-1996 22:27:16 EI+ Voltage SIX 70T
430.9729 F:4 Exp-.EPCUS
TRIANGLE LABS Texts23A-l TZI#39291R1 IMJ, TIME = 22:30
28:22 2S,44 -,<,.*, 29:01 29:15 -,a.-,-, 29:35
29:48
30:00
O.OEO
Time
28:12 28:24 28:36 28:48 29':00 29:12 29:24
FilesT966601 #1-443 Acq:31-OCT-1996 22:27:16 EI+ Voltage SIR 70T
479.7165 Fs4 Exp:EPCUS
TRIANGLE LABS Text:23A-l TLH39291R1 ISJ. TIME
IOCS 29s 12
29:36
22:30
-1 ! 1 1 , r-
25:48 30:00
28:12
28:24
28:36
28:48
29s 00
29:12
29:24
29t36
29s 48
30:00
-------
(5,3,1, 0.10*,2724.0,0. 00%,T,r) SxpsEPCUS
TRIANGLE LABS Text:23A-l TLI#39291X1 INJT. TIME * 22:30
100* A8.75E4
28:30 28:36 28:42 28:48 28:54 29sOO 29:06 2S-.12 29:18 29:24 29:30 S9-.36 29:42
F±le:T966601 #1-443 Acq:31-OCT-1996 22:27:16 EI+ Voltage SIR 701 N6iae;308
425.7737 F:4 BSUB(256,30, -3. 0) PKD(5,3,1, 0.101,1232. OrO,QQ*,T,r) Exp:EPCUS
TRIMBLE LASS Text:23A-l TEX13929Utl JK7. TIME = 22:30
1004
28:30 28:36 28:42 28:48 28:54 29:00 29:06 29:12 29:18 29:24 29:30 29:36 29:42
File:T966601 #1-443 AC9.-31-OCT-1996 22:27:16 EH- Voltage SIS 70T 2foiae:1506
435.8169 F:4 BSUB(256,30,~3.0) PKD(5,3,1, 0.10%, 6024 . 0, 0, 00\,T,T) Exp:EPCUS
TRIANGLE LABS Text:23A-l TLl#39291Rl IK7. TIME = 22:30
100* A2.
"-7.2E3
O.OEO
Time
-3.1E4
801
"-2.5E4
1.9E4
CJTO
Time
so:
eo:
401
201
9E7
I ! t I I I ! l"-'j •' I i" 'r"J T""T""T"! " j-fmy—•!!;!. YI -p- -fi-y.in..I t-"")i YI-I "t |""'y"T' f ;"-|""py"")-
28.-30 28:36 28:42 28:48 28:54 29:00 29:06 29:12 29:18 29:24 29:30
File:T966601 #1-443 Ac
-------
'ile:T966601 #1-443 Acq:31-OCT-1996 22:27:16 EH- Voltage SIS JOT KoiaesBlS
441.7428 Ps4 BSm(2S6,30,-3.0) PKD(7,2,3,0.10^,3260.0,0. 00%,F,F) EipiEPCUS
TRIAH5LE LABS Texts23A-1 TLI039291R1 JJKT. TIME ~ 22s30
1004 Al. 8E5
901
8 01
70J
601
sol
40;
30;
20;
w'l
0.
29:00 30i00 31s00 32:00
filesT966601 #1-443 Acq:31-OCT-1996 22s27il6 EH- Voltage SIR 70T Woi3e:9S2
443.7399 F:4 BSVS(256,30, -3. 0} PXD( 7,2, 3, 0,10%, 3908. 0,0.00%, F,F) Exp:EPCUS
TRIANGLE LABS Text:23A-l TLI#39291R1 JK7. TIME - 22:30
A1-33E4 A1.82E4 A2.21E4 , \ I '~'
\i>W^^^
33:00
32:00
29:00 30:00 31:00
F±le:T966601 #1-443 Acqs31-OCT-1996 22:27:16 EI+ Voltage SIR 70T
430,9729 F:4 Ezp:EPCUS
TRIANGLE LS.BS Texts23&-1 TLI#392S1R1 IKT. TIME =
1004. ~_ -. 10. »« *«.n, 31:03 31:35
33 s 00
22130
32:06 32:44 33:07
90.
a ol
701
601
501
401
301
201
101
0,
29:00 30:00 31:00 32:00
F±le:T966601 #1-443 Acq:31-OCT-1996 22:27:16 EI+ Voltage SIR JOT
513.6775 F:4 Efp:EPCnS
TRIANGLE LABS Tezt!23A-l TLI#39291R1 OKT. TIME "
1004 30 32
901
aoi
701
601
soi
401
301
201
101
0,
33:00
22:30
28; 55
31:43
32:42
33:05
8E4
3E4
8S4
3E4
9E4
4E4
9E4
4E4
SE3
8E3
OEO
Time
.4E7
3E7
1E7
OE7
6E6
1E6
7E6
3E6
,9E6
.4E6
OEO
Tan*
.6E4
,4E4
,3E4
,1E4
,5E3
,SE3
,3E3
.7S3
,2E3
,6E3
29:00
30:00
31:00
32:00
33 i 00
70
-------
*ilesT$666dl 91-443 Acqs31-OCT-lS96 22:27:16 ...... 1 1+
57.7377 F:4 BSm(256,30,-3.0) TXD(7,2,3, 0.10%,fl64. 0,
TRIANGLE LABS Text:23A-l XLH39291S1
1004 A2.02S5
32:06
31:36 31t42 31s48 31:54 32:00
File:T966601 #1-443 Acq:31-OCT-1996 22s27sl6 EI+ Voltage SIS 70T m>iae:356
459.7348 F:4 BSUB(256,30, -3.0) PKD(7,2,3,0.101>,1424 . 0,0. 00\,T,T) ExpsEPCVS
TSIAWSLE LABS Text:23A-l 15,1*39291X1 IKT. TIME = 22:30
100* A2.10E5
so:
31:36 31:42 31:48 31s54 32:00 32:06
File:T9SS601 01-443 Acg:31-OCT~1996 22:27:16 EI+ Voltage SIS 70T So±ae:223
469.7779 F:4 SSUB(256,30, -3. 0) Pm>(7,2,3, 0.101,892.0, 0. 00%,F,F) Etp:SPCOS
TRIANGLE LABS Text:23A-l ZLI#39291R1 JJKT. TIME = 22s30
100* A3__,J.2E7
801
T,r) ExptSPCUS
IJKT. TIME - 22:30
31:36 31:42 31:48 31:54 32:00 32:06
FilesT966601 #1-443 Acq:31-OCT-1996 22:27:16 EH- Voltage SIS 70T KaS.Be-.222
471.7750 F:4 BSUB(256,30,-3.0) PKD(7,2,3,0,1Q\,888.0,0.00*,F,F) Exp-.EPCVS
TRIANGLE LABS Teit:23A-l TLI#39291S1 IKT. TIME = 22:30
100% A3,7_2E7
31:36 31 1 4.2 31-48 31:54 32jOO
FilesT966601 #1-443 Acqt31-OCT-1996 22:27:16 EI+ Voltage SIR 70T
430.9729 T-.4 ExpiEPCUS
TRIANGLE LABS Text:23A-l TLI039291S1 ISJ. TIKE
32:06
BO:
so:
401
so:
o:
31-3S
00
32.-Off
S$-0. OEO
32:12 lime
32:12
1.1E7
.8.9E6
.6.7E6
.4.5E6
.2.2E6
.0 .OEO
32s 12 Time
r1.3E7
'.1.1X7
"-8.0E6
'-5.3E6
'.2.7E6
.O.OSO ,
32:12 Tim-
-1.4X7
'.1.1E7
-8.3E6
.5.5E6
'-2.8E6
o. oiro
Time
-------
tef, iass Flak-top
Height 5,81 udts Sp 296 cpt
EPCUS
D--T1B3186
a*
Systet file
tData file naie
« Resolution
Sroupnuiber
lonizabion
Switching
fef, masses
J 33! 3 388
X .332 I 378
I '334 U 378
PI 348 V 418
N 342
? ^4
I 330,3792 hm top
IteiglJt 4,45 uotts ';pan 280 p
-------
File:T966601 ttl-835 Acq:31-OCT-1996 22:27:15 EI+ Voltage SIR 70T Noise:2150
303.9016 F:2 BSUB(256,30,-3 . 0) PKD(7,3,I,0.10%,8600.0,0.00%,F,T) Exp:EPCUS
Sample Text:23A-l TLI#39291R1 INJ, TIME = 22:30 File Text:23A-l
100%. A3 ..98E5
A3.24E5 .
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0.
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1.3E5
1
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13:30
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13:36 13:42
12:54 13:00 13:06 13:12 13i18 13^24
File:T966601 #1-835 Acq:31-OCT-1996 22:27:16 EI+ Voltage SIR 70T Noise:1848
305.8987 F:2 BSUB(256,30,-3 . 0) PKD(7,3,1,0.10%,7392.0,0.00%,F,T) Exp:EPCUS
Sample Text:23A-l TLI#39291R1 INJ. TIME = 22:30 File Text:23A-l
100% A5.29E5
50-
0,
A9.03E3
A3.43E5
A3.19E5
.O.OEO
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TLI#39»
1.7E5
18.7E4
13:36
13:42
12:54 . 13:00 13:06 13:12 13:18 13:24 13:30
File:T966601 #1-835 Acq:31-OCT-1996 22:27:16 EI+ Voltage SIR 70T
315.9419 F:2 Exp:EPCUS
Sample Text:23A-l TLI#39291R1 INJ. TIME = 22:30 File Text:23A-l
100%, 13; 04
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Time
50_
12:54
TLI#39»
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T
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13:42 Time
File:T966601 #1-835 Acq:31~OCT~1996 22:27:16 EI+ Voltage SIR 70T
317.9389 F:2 Exp:EPCUS
Sample Text:23A-l TLI#39291R1 INJ. TIME = 22:30 File Text:23A-l TLI#39»
100%, 13,-33 _9.7E3
501
0.
12:54 12
13:07
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13:06 13:12
, - 1 - 1 - ! - 1 - 1 - ] - 1 - 1
13:18 13:24
13:30
13:36
13 ! 42
O.OEO
Time
\
-------
File:T966601 #1-835 Acq: 31-OCT-I^F96 22:27:16 EI+ Voltage SIR 70T Noise:2150
303.9016 F:2 BSUB(256,30,-3.0) PKD(7,3,1,0.10%,8600.0,0.00%,F,T) Exp:EPCUS
Sample Text:23A-l TLI#39291R1 INJ. TIME = 22:30 File Text:23A-l TLI#39»
7.8E4
13.9E4
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0
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14J42 14:48 14i54 15:00 15:06 15:12 15:18 15:24 15:30 Time
File:T966601 #1-835 Acq:31-OCT-1996 22:27:16 EI+ Voltage SIR 70T Noise:1848
305.8987 F:2 BSUB(256,30,-3.0} PKD(7,3,1,0.10%,7392.0,0.00%,F,T) Exp:EPCUS
Sample Text:23A-l TLI#39291R1 INJ. TIME = 22:30 File Text:23A-l TLI#39»
1001, ddfT87E5^ f _9.7E4
i2.62E5
501
0.
14.9E4
15:24
15:30
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Time
14:42 14:48 14:54 15:00 15:06 15:12 15:18
File:T966601 #1-835 Acq:31-OCT-1996 22:27:16 EI+ Voltage SIR 70T
315.9419 F:2 Exp:EPCUS
Sample Text:23A-l TLI#39291R1 INJ. TIME = 22:30 File Text:23A-l TLI#39»
lOOSs 9.1E6
14.6E6
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14! 42 14:48 14:54 15:00 15:06 15:12 15:18 15:24 15:30 Time
File:T966601 #1-835 Acq:31-OCT-1996 22:27:16 EI+ Voltage SIR 70T
317.9389 F:2 Exp:EPCUS
Sample Text:23A-l TLI#39291R1 INJ. TIME = 22:30 File Text:23A-l TLI#39»
100% . _1.2E7
501
—I - 1 - 1 - 1 - 1 - r — i - 1 - 1 - 1 - 1 - 1 - 1 - 1 - 1 - 1 - 1 - 1 - 1 - 1
14:42 14:48 14:54 15:00
1 - 1 - 1 - 1 - 1 - 1 - 1 — I - r - 1 - 1 - 1 - 1 - 1 - 1 - 1 - 1 - 1 - 1 - 1 - 1 - 1 - 1 — ! - 1
15:06 15:12 15:18 15:24 15:30
.6.0E6
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Time
-------
File:T966601 #1-835 Acq:31-OCT-1996 22:27:16 EI+ Voltage SIR 70T
319.8965 F:2 Exp:EPCUS
Sample Text:23A-l TLI#3929lRl INJ, TIME = 22:30 File Text:23A-l TLI#39»
100%, _ dk§7j4ElL> _2.0E4
0.
T
r - 1 - 1
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16:36 Time
16:00 16:06 16:12 16:18 16:24
File:T966601 #1-835 Acq:31-OCT-1996 22:27:16 EI+ Voltage SIR 70T
321.8936 F:2 Exp:EPCUS
Sample Text:23A-l TLIf3929lRl INJ. TIME = 22:30 File Text:23A-l TLI#39»
100%.
A7.19E4
50-1
0.
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16:00 16:06 16:12 16:18 16:24
File;T966601 #1-835 Acq:31-OCT-1996 22:27:16 EI+ Voltage SIR 70T
331.9368 F:2 Exp:EPCUS
Sample Text:23A-l TLIf3929lRl INJ. TIME =
100% 16^22
16:09
16:30
16:36 Time
22:30 File Text:23A-l TLI#39»
0.
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16:30
16:36 Time
16:00 16:06 16:12 16:18 16:24
File:T966601 #1-835 Acq:31-OCT-1996 22:27:16 EI+ Voltage SIR 70T
333.9338 F:2 Exp:EPCUS
Sample Text:23A-l TLI#39291R1 INJ. TIME = 22:30 File Text:23A-l TLI#39»
100%, i6-^2 .-1.0E7
i /* r\ r> / \
15.0E6
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16:36 Time
16:00
16:06
16:12
16:18
16:24
16:30
(
-------
cr
File:T966601 #1-835 Acg:31-OCT-1996 22:27:16 EI+ Voltage SIR 70T
339.8597 F:2 Exp:EPCUS
Sample Text:23A-l TLI#3929lRl
100% 20^27
INJ. TIME =
50
OJ
22:30 File Text:23A-l TLI#39»
_4.6E4
19:54
21:50
22:01
.2.3E4
.O.OEO
Time
20:00 21:00 22:00
File:T966601 fl-835 Acq:31-OCT-1996 22:27:16 EI+ Voltage SIR 70T
341.8567 F:2 Exp:EPCUS
Sample Text:23A-l TLI#3929lRl INJ. TIME = 22:30 File Text:23A~l TLIt39»
100% 20:27 _4.4E4
50
12.2E4
LlT.OEO
20:00 21:00 '22:00 Time
File:T966601 #1-835 Acq:31-OCT-1996 22:27:16 EI+ Voltage SIR 70T
351.9000 F:2 Exp:EPCUS
Sample Text:23A-l TLI#39291R1 INJ. TIME = 22:30 File Text:23A-l TLI#39»
100% 20; 50 _1.2E7
50:
0
21:49
T
.5.9E6
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Time
20:00 21100 22iOO
File:T966601 #1-835 Acq:31-OCT-1996 22:27:16 EI+ Voltage SIR 70T
353.8970 F:2 Exp:EPCUS
Sample Text:23A-l TLI#39291R1 INJ. TIME = 22:30 File Text:23A-l TLI#39»
100% 20:50 _7.7E6
50
21:49
20:00
21:00
22:00
.3.9E6
-O.OEO
Time
-------
File:T966601 #1-835 Acq:31-OCT-1996 22:27:16 EI+ Voltage SIR 70T
355.8546 F:2 Exp:EPCUS
Sample Text:23J^l__TLI#3929lRl
100%
INJ. TIME = 22:30 File Text:23A-l TLI#39»
5.0E4
22loQ
Time
21:00
File:T966601 #1-835 Acq: 31-OCT-1996 22:27:16 El-f- Voltage SIR 70T
357.8516 F:2 Exp:EPCUS
Sample Text:23A-l TLI#3929lRl INJ. TIME = 22:30 File Text:23A-l TLI#39»
100% rALQlEj) A7.07E4 -2 •6E4
50J / \ M .A tH3E4
O.OEO
21100 22100 23:00 '"'' Time
File:T966601 #1-835 Acq:31-OCT-1996 22:27:16 EI+ Voltage SIR 70T
367.8949 F:2 Exp:EPCUS
Sample Text:23A-l TLI#3929lRl INJ. TIME = 22:30 File Text:23A-l TLI#39»
100% 22;17
50.
0.
"1 r-
-i 1-
i^*"" • r
[
13.4E6
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-------
TLI Project: 39291rl
Client Sample: 23A-1
Method 23 TCDD/TCDF Analysis (DB-225)
Analysis File: X964233
Client Project:
Sample Matrix:
TLI ID:
Eastern Ridge Lime Facility
M23TRAIN Date Received: 10/19/96
143-23-lA,B Date Extracted: 10/21/96
Date Analyzed: 11/01/96
Spike File: SPC2NF08
ICal: XF21266
ConCal: X964226
Sample Size:
Dry Weight:
GC Column:
1.000
n/a
DB-225
Dilution Factor: n/a
Blank FUe: T966616
Analyst: JF
% Moisture: n/a
% Lipid: n/a
% Solids: n/a
2,3,7,8-TCDF
0.03
0.80
20:22
3C)2-2,3,7,8-TCDF
7,4
93.0
40%-130%
0.79
20:22
13Cl2-l,2,3r4-TCDD
0.80
19:25
Data Reviewer:
Page 1 of 1
11/11/96
C2NFJPSR*1.14. LARS 6.08 00
Triangle Laboratories, Inc.®
801 Capitate Drive • Durham, North Carolina 27713
Phone: (919) 544-5729 • Fax: (919) 544-5491
Printed: 16:12 11/11/96
82
-------
Initial —.Date —
Data Review By:
KVl^ iL/JL/laS Calculated Noise
Area:
The Total Area for each peak with an ion abundance ratio outside
racio limits has been recalculated according to method requirements.
7.00
Page No. 1
11/01/96
Compound/
M_Z QC. Log Omit Why
Listing of X964233B.db£
Matched GC Peaks / Ratio / Ret. Time
.RT. OR Ratio Total.Area.,. Area.Peak.1.. Area.Peak.2.. Rel.RT Compound,Name.. ID.
TCDF
304-306 DC NL 0:
16
DC SN 16
17
17
17
17
17
17
18
18
18
DC SN 18
18
DC SN 18
19
19
19
19
19
20
20
20
20
20
21
DC SN 22
DC SN 22
0.65-0.89
:00
:13
:32
:08
;14
:20
:33
:47
-.56
:01
:12
:22
:30
:43
:SS
:07
:22
;34
:44
:S2
:16
:22
:32
:46
:52
:31
:05
:10
RO
RO
RO
RO
RO
RO
RO
RO
RO
RO
RO
RO
RO
0
1
0
0
0
0
0
0
0
1
0
0
0
0
0
1
0
0
1
0
0
0
0
1
0
0
0
0
.47
.02
.78
.80
.64
.89
.77
.70
.84
.02
,77
.72
.53
.78
.60
.24
.79
.81
.17
.59
.94
.80
.78
.01
.86
.75
.41
.56
304-306 22 Peaks
13C12-TCDF
316-318 DC NL 0
DC WL 19
DC WL 19
19
20
20
DC WH 22
:00
-.06
:20
:58
i22
:53
:07
0.
RO
RO
RO
RO
8
235
3
196
115
340
141
124
231
48
392
188
1
371
4
121
202
125
28
111
99
109
123
69
101
52
5
1
3,529
.10
.59
.68
.75
.34
.71
.31'
.21
.27
.56
.30
.38
.23
.22
.48
.98
.76
.63
.24
.05
.30
.12
.37
.17
.08
.58
.55
.61
.92
135
87
50
160
61
51
105
28
170
79
162
85
89
56
18
48
52
48
53
39
46
22
.89
.66
.35
.42
.43
.26
.69
.05
.20
.02
.97
.31
.54
.28
.63
.56
.78
.47
.88
.43
.76
.46
132.
109.
78.
180.
79,
72.
125.
27.
222.
109.
208.
69.
113.
69.
15.
81.
56.
60.
69.
39,
54.
30,
65-0.89
5
1
0
3
0
0
0
.53
140
.93
.50
.79
.71
.77
316-318 3 Peaks
ah.
1
82
150
26
27,285
218
375
27,529
"stro • ITVTI
.41
.29
.38
.18
.30
.31
.91
.79
il? / TV
51
12,018
90
"TYri 1?/\1 1 n
.76
.00
.41
0.788-1.094
97
09
23
29
88'
95
58
37
10
36
25
06
22
35
99
63
,06
.65
,49
,12
,32
,12
0.
14.79
15,267.
127
.30
.90
0.000
0.796
0.812
0.841
0.846
0.851
0.862
0.873
0.881
0.885
0.894
0.902
0.908
0.919
0.929
0.939
0.951
0.961
0.969
0.975
0.995
1.000 2378-TCDF
1.008
1.020
1.025
1.056
1.084
1.088
951-1.049
0.000
0.938
0.949
0.980
1.000 13C12-2378-TCDF
1.025
1.086
AN
ISO
Triangle Laboratories, Inc.® Analytical Services Division
801 Capitals Drive • Durham, North Carolina 27713
Phone: (919) 544-5729 • Fax: (919) 544-5491
Printed: 17:38 11/0
-------
Page No.
11/01/96
Listing of X964233B,dbf
Matched GC Peaks / Ratio / Ret. Time
Compound/
M_Z QC.Log Omit Why
13C12-TCDD
332-334
DC
DC
DC
..RT. OK Ratio Total.Area... Area.Peak.1.. Area.Peak.2.. Rel.RT Compound,Name., ID,,
0.65-0.89
332-334
NL
SN
WH
4
0:
18
19
19;
19;
20
21
:00
:10
:13
:25
:39
;06
:37
RO
RQ
RO
RO
1
0
0
0
0
0
0
.13
.90
.78
.80
.62
.87
.92
Peaks
0.896-1.104
1.47 0.000
74.59 37.96 42.11 0.945
19,439.34 8,519.34 10,920.00 1.000 13C12-2378-TCDD IS1
10,571.50 4,697.52 5,873.98 1.010 13C12-1234-TCDD RSI
13.13 1.023
217.18 101.15 116.03 1.046
14.62 1.125
30,302.61
Column Description.
•Why" Code Description QC Log Desc.
M_Z -Nominal Ion Mass(es)
. .RT. -Retention Time (mnuss)
Rat.l -Ratio of M/M+2 Ions
OK -RO=Ratio Outside Limits
Rel.RT-Relative Retention Time
End of Report
WL-Below Retention Time Window
WH-Above Retention Time Window
SN-Below Signal to Noise Level
-------
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37
-------
>ile:X964233 #1-784 Acq: l-NOV-1996 16:41:36 OC BI+ Voltage SIM AutoSpec
303.9016 Exp:XCOHF_TT
Saople T»xt:23A-l TLI#39291rl File TextsTSIANCUJS LASS
lOCSt 18 12
16:00 17:00 18*00 15*00 20*00 21*00
Fil**arS64233 #1-784 Acq: l-HOV-1996 16:41:36 OC ET* Voltage SIR AutoSpec
3IS. 9419 Exp:XCONF_TT
Sasfle Text:23A-l TLI#39291rl File Text:TRIANOLE LABS
100*
16*00 17:00 18:00 15:00 20:00 21:00 22:00
Fil»:X964233 #1-784 Acq; l-NOV-1996 16:41:36 OC El* Voltage SIR AutOSpec
319.8965 ExpiXCOSF_TT
Sample Toxt:23A~l TLI#39291rl File Text:TRIANGLE LABS
10® 17," 01
80:
60:
401
20:
16:13
19:22
21.-31
22.-o
80.
eo:
401
20:
ol
20:22
SO:
60:
40:
201
ol
20:14
22:08
16:00 17:00 18:00 1S:00 20:00 21:00
File:X964233 #1-784 Acqt l-MOV-1556 16:41:36 OC JET* Voltage SIR AvtoSpec
331,9368 Exp:XCONF_TT
Sample Text:23A-l TLI#39291rl File Text:TRIANGLE LABS
IOCS 19113
sol
601
40:
20:
a- , ,
22sOO
16:00 17:00 18:00 15*00 20*00 21:00
File,-ZS64233 #1-784 Acqs l-SOV-1996 16:41:36 OC El* Voltage SIR AutoSpec
292,9825 Exp:XCONP_TT
Saaple Text:23A-1 TLI#39291rl File Text:TRIAKOLE LABS
10QS
80^
60J
40:
20:
0.
17:45
15.-13 15.-43 20.-15 20/50
22.-00
21.-3421.-S7
16:00 17:00 18:00 15*00 20*00 21:00
Fil«.-JTS64233 #1-784 Acqt l-SOV-1996 16:41:36 OC SIf Voltage SIR AutoSpec
330.9792 Exp:XCQNF_TF
Sample Text:23A-1 TLI#39291rl File Text:TRIANOLE LABS
16*40 17--23 17,5* 18:33 18:55 I9_j36.. 20;2320:4621:09 21:33
22*00
1003
so:
so:
40:
20:
o:
17.-23
ISiOQ
17:00
it tOO
iSlOO
20»00
21*00
22sOO
^2.9S5
.2. 3ES
.2-2ES
a.oso
^2.6E7
1.SS7
1.0E7
O.OEO
Timm
2.3ES
1.8SS
1.4E5
.S.2E4
a-,
riaie
_1.JE7
6. 4E6
.3.2E6
O.OES
Time.
.4. 6E7
.3.7E7
.2.8E7
.O.QEC
Tims
-.2.6E7
Ll.7F7
.cm
.O.OEO
Tim*
83
-------
Peak Locate Examination: l-NOV-1996:16:41 File:X964233
Experiment:XCONF_TT Function:! Reference:PFK
cr
CO
-------
TLI Project:
Client Sample:
39291rl
23A-2
Method 23 PCDD/PCDF Analysis (a)
Analysis File: T966602
Client Project:
Sample Matrix:
TLI ID:
Sample Size:
Dry Weight:
GC Column:
Eastern Ridge Lime Facility
M23TRAIN Date Received: 10/19/96
143~23-2A,B Date Extracted: 10/21/96
Date Analyzed: 10/31/96
1.000 Dilution Factor: n/a
n/a Blank File: T966616
DB-5 Analyst: BB
Spike File:
ICal:
ConCal:
% Moisture:
% Lipid:
% Solids:
SPX23708
TF53286
T966598
n/a
n/a
n/a
2,3,7,8-TCDD
1,2,3,7,8-PeCDD
1,2,3,4,7,8-HxCDD
1,2,3,6,7,8-HxCDD
1,2,3,7,8,9-HxCDD
1,2,3,4,6,7,8-HpCDD
1,2,3,4,6,7,8,9-OCDD
2,3,7,8-TCDF
1,2,3,7,8-PeCDF
2,3,4,7,8-PeCDF
1,2,3,4,7,8-HxCDF
1,2,3,6,7,8-HxCDF
2,3,4,6,7,8-HxCDF
1,2,3,7,8,9-HxCDF
1,2,3,4,6,7,8-HpCDF
1,2,3,4,7,8,9-HpCDF
1,2,3,4,6,7,8,9-OCDF
Total TCDD
Total PeCDD
Total HxCDD
Total HpCDD
Total TCDF
Total PeCDF
Total HxCDF
Total HpCDF
ND
ND
ND
ND
ND
0.18
0.62
0.07
ND
0.01
0.05
0.02
0.05
ND
0.20
0.06
0.61
0.21
0.06
0.12
0.34
0.40
0.04
0.17
0.42
0.01
0.02
0.02
0.02
0.02
0.01
0.02
^vwvmmvimixvtyfmmvftuyxtii
4
2
2
2
10
2
6
4
0.91
0.87
0.70
1.50
1.39
1.26
1.18
1.09
1,00
0.90
0.22
0.14
0.14
0.42
0.07
29:14 ~~
31:42
15:36
21:50
25:12
25:20
25:55 B__
28:18 ~~
29:33
31:46
Page 1 of 2
XZSTJSR. Yl.14, LARS 6.08.00
Triangle Laboratories, Inc.®
801 Capftola Drive • Durham, North Carolina 27713
Phone: (919) 544-5729 • Fax: (919) 544-5491
Printed: 16:03 11/11/96
no
-------
TLI Project:
Client Sample:
39291rl
23A-2
Method 23 PCDD/PCDF Analysis (a)
Analysis File: T966602
l3C12-2,3,7,8-TCDF
13CI2-2,3,7,8-TCDD
13Ci2-l,2,3J,8-PeCDF
13e,2-l,2,3,7,8-PeCDD
!3C,2-l,2,3,6,7,8-HxCDF
13Ci2-l»2,3,6»7,8-HxCDD
13e,2-l,2,3,4,6,7,8-HpCDF
l3Cu-lA3A6,7,8-HpCDD
13Ci2-l,2,3,4,6,7,8,9-OCDD
5.3
5.5
5.0
4.6
5.1
6.0
5.9
6.1
11.5
66.8
69.2
62.7
57.8
64.0
75.3
73.5
76.0
71.7
40%-130%
40%-130%
40%-130%
40%-130%
40%-130%
40%-130%
25%-130%
25%-130%
25%-130%
0,75
0.80
1.54
1.50
0.48
0.43
1.04
0.84
15:35
16:21
20:50
22:17
25:19
26:10
28:18
29:14
31:41
!3Ci2-2,3,4,7,8-PeCDF
!3Ci2-l,2,3,4,7,8-HxCDF
!3C12-l,2,3,4,7,8-HxCDD
l3C,2-l,2,3,4,7,8,9-HpCDF
4.5
4.4
4.9
4.3
5.0
111
111
123
107
126
70%-140%
70%-140%
70%-140%
70%-140%
70%-140%
1.48
0.49
1.22
0.42
16:23
21:49
25:12
26:05
29:32
13Ci2-l,2(3,7,8,9-HxCDF
13e,2-2,3,4,6,7,8-HxCDF
3.4
3.2
84.6
80.6
40%-130%
40%-130%
0.48
0.48
26:40
25:55
l3e,2-l,2,3,4-TCDD
13Cn-l,2,3,7,8,9-HxCDD
0.79
1.20
16:08
26:28
Data Reviewer:
11/11/96
Page 2 of 2
X2J7JPSR vl.14, LARS 6.08.00
Triangle Laboratories, Inc.®
801 Capitola Drive • Durham, North Carolina 27713
Phone: (919) 544-5729 • Fax: (919) 544-5491
Printed: 16:03 11/11/96
31
-------
TLI Project: 39291rl
Client Sample: 23A-2
Toxicity Equivalents Report
Analysis File: T966602
Client Project:
Sample Matrix:
TLI ID:
Sample Size:
Dry Weight:
GC Column:
Eastern Ridge
M23TRAIN
143-23-2A,B
1.000
n/a
DB-5
Lime Facility
Date Received:
Date Extracted:
Date Analyzed:
Dilution Factor:
Blank File:
Analyst:
10/19/96
10/21/96
10/31/96
n/a
T966616
BB
Spike File:
ICal:
ConCal:
% Moisture:
% Lipid:
% Solids:
SPX23708
TF53286
T966598
n/a
n/a
n/a
2,3,7,8-TCDD
1,2,3,7,8-PeCDD
1,2,3,4,7,8-HxCDD
1,2,3,6,7,8-HxCDD
1,2,3,7,8,9-HxCDD
1,2,3,4,6,7,8-HpCDD
1,2,3,4,6,7,8,9-OCDD
TOTAL PCDD
2,3,7,8-TCDF
1,2,3,7,8-PeCDF
2,3,4,7,8-PeCDF
1,2,3,4,7,8-HxCDF
1,2,3,6,7,8-HxCDF
2,3,4,6,7,8-HxCDF
1,2,3,7,8,9-HxCDF
1,2,3,4,6,7,8-HpCDF
1,2,3,4,7,8,9-HpCDF
1,2,3,4,6,7,8,9-OCDF
TOTAL PCDF
0.01
0.02
0.02
0.02
0.02
0.18
0.62
0.02
0.01
0.01
0.05
0.02
0.05
0.02
0.20
0.06
0.61
x
x
X
X
X
X
X
X
X
X
X
X
X
X
X
X
X
1
0.5
0.1
0.1
0.1
0.01
0.001
0.1
0.05
0.5
0.1
0.1
0.1
0.1
0.01
0.01
0.001
0.01
0.01
0.002
0.002
0.002
0.0018
0.00062
0.0284
0.002
0.0005
0.005
0.005
0.002
0.005
0.002
0.002
0.0006
0.00061
0.0247
Total EPA TEFs, 1989a: 0.0531 ng
Page 1 of 1
TEFPR V5.08, LARS 6.06.00
Triangle Laboratories, Inc.®
801 Capitola Drive « Durham, North Carolina 27713
Phone: (919) 544-5729 • Fax: (919) 544-5491
Printed: 16:21 11/11/96
-------
Initial
Date—
/ // / /P Calculated Noise Area:
Data Review By;
The Total Area for each peak with an ion abundance ratio outside
ratio limits has been, recalculated according to method requirements.
3.78
Page No.
11/11/96
Listing of T966602B.dbC
Matched GC Peaks / Eatio / Ret. Time
Compound/
M_Z.... QC.Log Omit Why ..FT. OK Eatio Total,Area... Area.Peak.1.. Area,Peak.2.. Rel.RT Compound.Name.. ID.
TCDF
304-306
H
M
H
M
M
K
K
304-306
13C12-TCDF
316-318
316-318
TCDD
320-322
A
A
A
320-322
37C1-TCDD
328
328
DC NL 0:00
13:04
13:24
13:34
13:50
14:05
14:24
14:39
14:53
15:11
15:36
16:04
16:16
12 Peaks
DC NL 0:00
14:38
15:11
15:35
16:04
4 Peaks
DC NL 0:00
14:00
DC SN 14:09
14:19
DC SN 14:34
15:10
DC SN 15:19
16:08
16:16
5 Peaks
DC NL 0:00
14:57
16:23
2 Peaks
0.65-0.89
RO 1.33
RO 0.53
0.88
0.67
0.76
0.77
0.75
0.70
0.79
0.80
0.70
0.87
RO 1.70
0.65-0.89
0.69
0.66
0.83
0.75
RO 0.50
0.65-0.89
RO 1.77
0.77
RO 1.25
0.67
RO 1.16
0.73
RO 0.40
RO 0.61
0.81
0,828-1.138
4.73
20.23
17.47
10.02
74.90
57.43
43.70
37.36
65.10
14.67
66.00
9.08
2.62
418.58
3,95
41.61
20.36
7,338.37
58.52
7,458.86
: TCDF / TCDD
2.07
107.08
1.50
49.49
2.05
28.30
0.94
9.22
14.98
209.07
0.89
59.49
3,276.32
3,335.81
8.80
8.18
4.03
32.29
25.05
18.70
15.36
28.70
6.52
27.20
4.22
2.52
16.59
9.23
3,146.74
25.57
46.71
19.88
11.90
4.01
6.69
59.49
3,276.32
16.60
9.29
5.99
42.61
32.38
25.00
22.00
36.40
8.15
38.80
4.86
1.48
0.
25.02
11.13
4,191.63
50.81
0.
60.37
29.61
16.40
6.56
8.29
0.
0.000
0.839
0.860
0.871
0.888
0.904
0.924
0.940
0.955
0.974
1.001 2378-TCDF AN
1.031
1.044
936-1.064
0.000
0.939
0.974
1.000 13C12 -2378-TCDF ISO
1.031
846-1.086
0.000
0.856
0.865
0.876
0.891
0.928
0.937
0.987
0.995
878-1.122
0.000
0.914
1.002 37C1-TCDD SOR1
Triangle Laboratories, inc.® Analytical Services Division
801 Cap'rtola Drive • Durham, North Carolina 27713
Phone: (919) 544-5729 • Fax: (919) 544-5491
Printed: 15:51 11/11/96
33
-------
Page No.
11/11/96
Listing of T9666Q2B.dbf
Matched GC Peaks / Ratio / Ret. Time
Compound/
M_2..,. QC.Log Omit Why ..RT. OK Ratio Total.Area... Area.Peak.1.. Area.Peak.2.. Rel.RT Compound.Name.. ID..
13C12-TCDD
0.65-0.89
0.878-1.122
332-334
332-334
PeCDF
340-342
D
D
M
D
M
D
D
D
M
340-342
13C12 -PeCDF
352-354
352-354
PeCDD
356-358
M
M
D
M
DC
DC
D
DC
D
D
D
D
DC
D
DC
DC
DC
DC
DC
DC
DC
DC
D
DC
NL
4
NL
SN
SN
SN
SN
SN
SN
SN
SN
SN
SN
SN
SN
4
NL
6
NL
SN
SN
SN
SN
0:00 RO
15:10 RO
16:08
16:21
16:46
Peaks
1.
0:00 RO
18:01 RO
18:41 RO
19:28 RO
19:39
19:54
20:28 RO
20:44 RO
20:53 RO
21:03 RO
21:16 RO
21:36 RO
21:41 RO
21:50
22:00 RO
22:45 RO
22:50
Peaks
1.
0:00 RO
19:37 RO
20:23 RO
20:50
21:03 RO
21:15
21:49
Peaks
1,
0:00 RO
19:54 RO
20:16 RO
20:27 RO
20:53
21:07
21:21
21:55 RO
22:03
2.47
0.45
0,79 4,
0.80 6,
0.70
10,
32-1.78
0.62
1.09
0.18
2.24
1.69
1.70
1.27
0.74
0.76
5.06
0.86
0.95
2.00
1.50
0.98
0.56
1.59
32-1.78
0.75
0.76
0.79
1.54 6,
3.55
1.57
1.48 3,
10,
.32-1.78
2.39
1.31
0.13
0.78
1.41
1,72
1.37
1.98
1.56
4,44
13.38
339.94
297.99
70.24
721.55
5
1,912
2,806
28
.82
.39
.08
.84
12.94
2,427.55
3,491.91
41.40
0
0
0
1
1
.000
.928
.987 13C12-1234-TCDD
.000 13C12-2378-TCDD
.025
RSI
IS1
2.01
11.57
0.30
5.64
28.00
6.77
19.41
2.11
3.14
1.25
2.34
1.25
0.38
9.31
9.30
1.15
1.58
66.02
l'.09
14.77
8.86
569.61
12.89
17.61
713.78
337.52
>«/T'!l? /
'ew»>r /
1.63
31.75
0.59
1.50
22.53
3.75
13.44
10.33
1.10
17
11
5
5
8
5
3,982
17
10
2,214
.60
.80
.58
.65
.97
.40
.44
.94
.76
.04
0.
10.40
9.29
3 .73
5.75
0.
11.82
6.80
2,587.17
5.06
6.85
1,499.74
855'
0
0
0
0
0
0
0
0
1
1
1
1
1
1
1
1
1
-1.112
.000
.865
.897
.934
.943
.955
.982
.995
.002 12378-PeCDF
.010
.021
.037
.041
.048 23478-PeCDF
.056
.092
.096
AN
AN
808-1.192
0
0
0
1
1
1
1
.000
.942
.978
.000 13C12-PeCDF 123
.010
.020
.047 13C12 -PeCDF 234
JS2
SOR2
19
13
7
8
.30
.20
.78
.03
0.
14.70
9.33
5.66
4.05
885-1.034
0
0
0
0
0
0
0
0
0
.000
.893
.909
.918
.937
.948
.958
.984
.990
Triangle Laboratories, Inc.® Analytical Services Division
801 Capitola Drive • Durham, North Carolina 27713
Phone: (919) 544-5729 • Fax: (919) 544-5491
Printed: 15:51 11/11/96
34
-------
Page No.
11/11/96
Listing of T966602B.dbf
Matched GC Peaks / Ratio / Ret. Time
Compound/
M_Z.... QC.Log Omit Why . .RT. OK Ratio Total. Area... Area. Peak. 1.. Area. Peak. 2. . Rel.RT Compound.Name.. ID.
D
356-358
13C12-PSCDD
368-370
368-370
HxCDF
374-376
H
D
H
M
374-376
13C12 -HxCDF
384-386
384-386
HxCDD
390-392
M
M
DC SN 22:19 RO 0 .50
DC SN 22:24 RO 1.12
DC SN 22:32 RO 4.13
D SN 22:40 RO 1.23
DC SN 22:54 RO 0.67
4 Peaks
1.32-1.78
DC NL 0:00 RO 14.00
22:17 1.50
22:28 1.69
22:37 RO 0.43
22:54 RO 0.40
4 Peaks
_« «.**«-«— ««*__.. *. iV\*"rtn» •
1.05-1.43
DC NL 0:00
24:07
24:16
25:12
25:20
DC SN 25:26
D SN 25:37
25:55
26:45
6 Peaks
1.
1.
1.
1.
1.
RO 0.
RO 0,
1.
1.
24
18
42
39
26
54
76
18
16
1.84
1.05
1.63
2.68
1.32
78.05
0.18
3,556.54
330.22
2.96
2.41
3,892.13
'Dai""*!"1!!"! /
! JnSsv.'.liftU /
4.56
10.76
17.56
30.08
13.15
0.89
2.80
28.60
6.47
106.62
2,131.43
207.53
1.81
1.47
1.001 12378-PeCDD
1.005
1.011
1.017
1.028
0.821-1.179
0.000
1,425.11 1.000 13C12-P6CDD 123
122.69 1.008
4.18 1.015
3.66 1.028
5.
10.
17.
7.
15.
3.
83
30
49
33
50
48
4.
7.
12.
5.
13.
2.
0.43-0.59
DC NL 0:00
24:05
24:14
25:12
25:19
25:30
25:55
DC SB 26:05
26:40
26:55
8 Peaks
RO 0.
RO 0.
0.
0.
0.
0.
63
60
59
49
48
47
0.48
RO 2.94
0.48
RO 1.56
1,05-1.43
DC NL 0 : 00
DC SN 24:39
24:44
DC SS 25:03
DC SN 25:07
25:15
25:30
RO 0
RO 0
RO 0
RO 0
RO 0
1
1
.62
.44
.98
.39
.78
.36
.13
2.59
14.13
10.05
2,571.02
4,468.20
8.02
2,667.90
1.67
2,277.61
2.55
12,019.48
* HxCD? /
2.28
0.33
8.24
0.31
0.63
47.22
15.11
5.
3.
849.
1,448.
2.
869.
743.
2.
62
74
52
31
58
13
.28
,63
9.
6.
1,721.
3,019.
5.
1,798.
1,534.
1.
AN
IS3
0.945-1.064
93
26
59
82
10
99
0.
0.
0.
0,
1,
1.
1.
1,
1.
000
.953
,959
,995 123478-HxCDF
,001 123678-HxCDF
,005
.012
.024 234678-HxCDF
.057
AN
AN
AN
0.842-1.158
35
31
50
89
44
77
33
69
0
0
0
0
1
1
1
1
1
1
.000
.951
.957
.995 13C12-HXCDF 478
.000 13C12 -HxCDF 678
.007
.024 13C12-HXCDF 234
.030
.053 13C12 -HxCDF 789
.063
SUR3
IS4
ALT2
<1
4.56
27
8
.17
.01
0.
4.67
20.05
7.10
939-1.017
0
0
0
0
0
0
0
.000
.942
.945
.957
.960
.965
.975
Triangle Laboratories, Inc.® Analytical Services Division
801 Captela Drive • Durham, North Carolina 27713
Phone: (919) 544-5729 • Fax: (919) 544-5491
Printed: 15:51 11/11/96
35
-------
Page No. 4
11/11/96
Compound/
M_Z.... QC.Log Omit Why
Listing of T966602B,dbf
Matched GC Peaks / Eatio / Ret. Time
,.RT. OK Ratio Total.Area... Area.Peak.1.. Area.Peak.2.. Rel.RT Compound.Name.. ID.
DC SN 25:39
D
390-392
13C12-HXCDD
402-404
402-404
HpCDF
408-410
408-410
13C12-HpCDF
418-420
418-420
HpCDD
424-426
424-426
13C12 -HpCDD
436-438
436-438
DC SN 25;
DC SN 25;
DC SN 26:
D SN 26
DC SN 26:
DC SN 26-
:42
:46
:06
ill
:15
:28
RO
RO
RO
RO
RO
RO
RQ
2.73
0.80
4.93
1.68
1.63
0,35
5.00
3 Peaks
DC NL 0
26
26
26
26
:00
:05
:10
:28
:40
1.
RO
4 Peaks
DC NL 0
28
28
28
DC SN 28
29
:00
:18
:32
:40
:56
:33
0.
RO
05-1.43
1.10
1.22
1.24
1.20
0.40
88-1.20
1.07
1.09
1.06
1,18
0.36
1.00
4 Peaks
DC NL 0
28
DC SN 28
29
:00
:18
:41
:32
0.
RO
RO
2 Peaks
DC NL 0
28
DC SN 28
29
DC WH 29
:00
:36
:47
:14
:26
0,
RO
RO
,37-0.51
1.15
0.43
0.18
0,42
.88-1.20
1.07
0.88
2.46
0.91
3.51
2 Peaks
DC NL 0
28
29
:00
:36
:14
0
RO
RO
.88-1.20
1.35
0.79
1.04
2 Peaks
1.
1.
0.
1.
4.
0.
1.
70.
48
07
34
05
37
70
25
57
0
0
0
0
1
1
1
.980
.982
.985
.997
.001
.003
.011
123478-HxCDD
123678-HxCDD
123789-HxCDD
AN
AN
AN
0.962-1.038
3.
1,974.
4,105.
2,890.
4.
8,975.
2,
156.
48.
50,
42
13 1,082.95
71 2,275.35
46 1,574.96
79 2.67
09
57
03 81.31
88 25.14
27 27.22
891.18
1,830.36
1,315.50
6.62
0.
74.72
23.74
23.05
0.91
28.
284.
3.
3,489.
2.
1,737.
5,226,
99 14.51
,17
17
,20 1,049.61
,36
.27 514.36
,47
14.48
0.
2,439.59
1,222.91
0.
1.90
68,
,16 31.92
36.24
1.20
71,
.34 33.97
37.37
0.88
0
0
1
1
1
.000
.997
.000
.011
.019
13C12-HXCDD 478
13C12-HXCDD 678
13C12-HXCDD 789
SOR4
IS5
RS2
995-1.051
0
1
1
1
1
1
929
0
1
1
1
.000
.000
.008
,013
.022
.044
1234678-HpCDF
123 47 89 -HpCDF
AN
AN
-1.141
.000
.000
.014
.044
13C12 -HpCDF 678
13C12-HpCDF 789
IS6
SOR5
973-1.006
0
0
0
1
1
.000
.978
.985
.000
.007
1234678-HpCDD
AN
139.50
3
6
3,382
3,389
.40
.92 3.53
.98 1,724.23
.90
0.
966-1,034
0
4.46 0
1,658.75
1
.000
.978
.000
13C12-HpCDD 678
IS7
Triangle Laboratories, Inc.® Analytical Services Division
801 Capitola Drive • Durham, North Carolina 27713
Phone: (919) 544-5729 » Fax: (919) 544-5491
Printed: 15:51 11/11/96
36
-------
Page No.
11/11/96
Listiug of T966602B.dbf
Matched GC Peaks / Ratio / Ret. Time
Compound/
M_Z.... QC.Log Omit why ..RT. OK Ratio Total.Area... Area.Peak.1.. Area.Peak.2.. Rel.RT compound.Name,- ID.,
OCDF
442-444
442-444
Above: HpCDD / Octa-CDD and CDF Follows
0.76-1.02
DC NL 0:00 RO 1.16 2.91
DC SN 29:14 1.02 2,28
31:46 0.90 224.67
1 Peak 224,67
106.60
0.874-1.126
0.000
0.923
118.07 1.003 OCDF
OCDD
458-460
458-460
0.76-1.02
DC NL 0:00 0.84 1.60
31:42 0.87 197.50
1 Peak 197.50
91.99
0.874-1.126
0.000
105.51 1.001 OCDD
AN
13C12-OCDD
470-472
470-472
DC NL
0.76-1.02
0:00 0.87
31:41
1 Peak
0.84
0.86
4,987.48
4,987.48
2,277.08
0.995-1.006
0.000
2,710.40 1.000 13C12-OCDD
IS8
Column Description.
•why" Code Description QC Log Desc.
M_Z -Nominal Ion Mass(es)
..RT. -Retention Time (mm:ss)
Rat.l -Ratio of M/M+2 Ions
OK -RO=Ratio Outside Limits
Rel.RT-Relative Retention Time
End of Report
WL-Below Retention Time Window
WH-Above Retention Time Window
SN-Below Signal to Noise Level
-------
en
?ile:T9666Q2 #1-835 Acq:31-OCT-1996 23:05:06
319.8965 F:2 Exp:EPCUS
Sample Text:23A-2 TLI#39291R1
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331.9368 F:2 Exp:EPCUS
Sample Text:23A-2 TLI#39291R1 INJ. TIME = 23:08 File Text:23A-2 TLI#39»
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Sample Text:23A-2 TLI#3929lRl INJ. TIME = 23:08 File Text:23A-2 TLI#39»
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TXIANSLE LABS Text:23A-2 TLU39291X1 JKT. TIME = 23: OS
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TRIANGLE LASS Text:23A-2 TLI#39291X1 INJ~. TIME- 23:08
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TRIANGLE LABS Text:23A-2 TLH392S1S1 IJfJ". TIME = 23:08
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TRIANGLE LASS Text:23A-2 TLI039291X1 IJKT. TIME
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TSIANGLE LABS Texti23A-2 TZI#39291X1 IKT. TIME - 23:08
100J>
18:00
4E6
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Time
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13:00
14:00
15:00
16: 00
17:00
18:00
-------
FilesT966602 #1-835 Acqs31-OCT-1996 23:05:06 EH- Voltage SIS JOT Noise: 1034
319.8965 Fs2 BSVB(256,30, -3 .0) J?JO>(5,3,1, 0.101,4136. 0,0. 00%,J-,f; Exp:EPCUS
TXIAHSLE LABS Text:23A-2 TLI#39291X1
1003
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40:
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JJKT. TIME - 23:08
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17:00 ' ' ' ' ' 18:00 Time
J*ile: 2"$Se« 02 #1-835 Acqt3l-OCT-1996 23:05:06 EI+ Voltage SIS JOT Noiaes583
321.8936 T:2 BSV3(256,30, -3.0) PKD(5,3,1, 0.10\,2332. 0,0.00%, t,T) Exp:EPCUS
TSIANSLS LABS Teits23A-2 TLH39291S1
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331.9368 F-.2 BSUB(256,30,-3.0) PKD(5,3,1,0 .10\,123J2.0,0 .00*,F,F) Exp-.EPCUS
TRIANGLE LABS Text:23A-2 TLI#39291R1
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File:T966602 #1-835 Acqs3l-OCT-1996 23:05:06 EH- Voltage SIS JOT Noiae-,1253
333.9338 F:2 BSUB(256, 30, -3 . 0) PKD(5, 3,1, 0.10%, 5012. 0, 0. 00%, F,F) Exp:EPCUS
TRIANGLE LABS Texts23A~2 TLI#39291R1
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327.8847 F:2 BSUB( 256,30, -3. 0) PKS( 5,3,1, 0.10%, 1784. 0, 0. 00%, F,F) Exp:EPCUS
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-------
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39.8597 Fs2 BSOS(25S,30,-3.0) tXD(S,3,l,0.1Q*,2436.0,0.00*,T,f) ErpsEPCUS
TRIANGLE LABS Text; 23 A- 2 TLI#3929lSl IKT. TIME - 23 1 08
OOS • Al . 74E5
18:00 19:00 20:00 21:00 22:00 23:00
File:T966602 #1-835 Acqs31-OCT-1996 23:05:06 EI+ Voltage SIJR 701 Koiee:988
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20:
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Time
18': 00 19'sOO 20:00 21:00 22:00
file:T966602 #1-835 Acq:31-OCT~1996 23:05:06 XI + Voltage SIS 70T !Toiae:328
351.9000 F:2 BS0B(256, 30, -3. 0) PKD(5, 3,1, 0.101,1312. 0, 0, 00%,F,r) Exp:EFCUS
TRIANGLE LABS Text:23A-2 TX.H3S291X1 HKT. TIME - 23:08
1003, ' A3.98E7
23:00
80J
601
401
201
A2.21E7
18:00 ISsOO 20.-00 21tOO 22:00
File:T966602 #1-835 Acqi31-OCT-1996 23:05:06 EI+ Voltage SIR 70T lToiaa:440
353.8970 F:2 BSOS(256, 30,-3 .0) PKDfS, 3,1,0.10\, 1760.0,0.00\,F,F) EipsEPCUS
TRIANGLE LABS Teit:23A-2 TLI#39291Rl ItKT. TIME = 23:08
A2.59E7
23: 00
ao:
sol
40:
201
A1.50E7
18:00 19:00 20:00 21:00 22:00
FilesTS66602 il-835 Ac
-------
Tile:T966602 #1-835 Acq:31-OCT-l996 23:05:06 EI+ voltagre SIX JOT Noises 767
355.8546 F:2 BSOS(256,30,-3.0) PKD(5r3rl,0.10*,3068.0,0.00\,F,F} ExpsEPCVS
TRIANGLE LABS Text:23A-2 TLI#39291R1 IK7. TIME - 23s OB
100i,R1.76E5
80.
20:00 21:00 22:00
File:T966602 #1-835 Acq:31-OCT-1996 23:05:06 EI+ Voltage SIS 70T Jfo.sure.-322
357.8516 F-.2 BSUB(256,30, -3.0) PXD(5,3,1,0.10%, 1288. 0,0. 00%,F,F) Eip:EPCUS
TRIANGLE LABS Text:23A~2 TLI#39291X1 IMJ. TIME - 231
1004 . A5.6SE4
23:00
08
20:00 21:00 22:00
F±le:T966602 #1-835 Ac%t31-OCT-1996 23:05:06 EI+ Voltage SIR 70T Noiaes489
367.8949 F:2 BSVS(256,30r-3.0) PKD(5,3,1, 0.10%,1S56, 0, 0. 00%,f,F) Exp:EPCUS
TRIANGLE LABS Text:23A-2 TLI#39291R1 INJ. TIME = 23:08
1004 A2.J.3E7
so:
so:
40:
20:
23 i 00
2.08E6
20:00 21:00 22:00
FilesT966602 #1-835 Acq:31-OCT-1996 23:05:06 EI+ Voltage SIS 70T lfoiae:37
369,8919 Fs2 BSUS(256,30,-3.0} PKD(5,3,1, 0.10%,148, 0, 0.00%,?,F) ExpiEPCUS
TRIANGLE LASS Texti23A-2 TLI#39291S1 X1KJ. TIKE = 23:08
1004 A1.43E7
801
601
401
201
23 : 00
20s00 21:00 22:00
F±lesT966602 #1-835 Acqt31-OCT-1996 23:05:06 EI+ Voltage SIS 70T
330.9792 F:2 Exp:EPCUS
TRIANGLE LABS Text:23A-2 TLH39291X1 IKT. TIME
100$ 20_>VL 2&il?^ 21:09 21:26 22:10
801
601
401
201
23 : 00
201 00
21:00
22:00
23iOO
.5. 6E6
.4.5E6
.3. 4E6
.2.2E6
.1. 1E6
.O.OEO
Time
.3. 8E6
.3. OE6
.2.3E6
.1.5E6
.7.6E5
.O.OEO
Time
.3.6E7
.2.9E7
.2.2E7
.1.4E7
.7.2E6
.O.OEO
Time
1-2
-------
'±lesT966S02 #1-505 Acq:31-OCT-1996 23:05s06 EI+ Voltage SIS 701* Noise: 1258
373.8208 Tt3 BSUB(256r30,-3.0) FKD(5,3,1, 0.101,5032. 0,0.00%, f,r) ExptEPCUS
TRIKNSLE LRBS Text:23A-2 TLH39291S1 INJ". TIME = 23s 08
24s 00 25:00 26:00
f±lesT966602 #1-505 Aoq s31-OCT-1996 23:05:06 EI+ Voltage SIR 70T Noises 1019
375.8178 Fs3 BSm(256,30,-3.0) fKI>(5, 3,1, 0 .101,4076.0,0 ,00*,F, f) ExptSPCOS
TRIANGLE LABS Teit:23A-2 TLI#39291X1 IKT. TIME = 23:08
1003| A1.21E5
24s00 25:00 26:00
File:T966602 #1-505 Acq:31-OCT-1996 23:05:06 El* Voltage SIS 70T Koiaet542
383.8639 F:3 BSU$(2S6,30, -3.0) PKD(5,3rl, 0.10%, 2168.0,0. 00%,F,f) Exp:EPCUS
TRIANGLE LABS Text:23A-2 TLI#39291S1 UKT. TIME = 23:08
1004 A1.45E7
27:00
A1.26E5
I
A2.0SE4
J \A6.91E3 R1'J?E4
f*- ^^f&KAW^M^^^vTfS^^
27s 00
ao
sol
OJ
AB.69E6
A7.43E6
24:00 25:00 26:00
File:'T966602 #1-505 Aoq:31-OCT-1996 23:05:06 EI+ Voltage SIS 70T SOieesBSO
385.8610 r:3 BSUB(256,30, -3.0} PKD(5,3,1, 0.101,3440. 0, 0. 00%,F,F) Elp:EPCaS
XXIANSLE LABS Texts23A-2 TLI#39291X1 ItKT, TIKE = 23:08
1003, A3.02E7
27:00
801
sol
401
201
Al.80E7
A1.53E7
24:00 25:00 26:00
fileiT966602 #1-505 Acg:31-OCT-1996 23:05:06 EI+ Voltage SIR JOT
392.9760 F:3 Exp:EPCGS
TRIANGLE LABS Text:23A-2 TLI&39291S1 IKT. TIME
25:02 25:1725:28 25:44
^\*VAA/N/W\'W~W--V" ^r—*• T-"1\/\^'VVV" « -- -
80J
so:
40!
201
0,
27:00
24:00 25:00 26:00
F±le:T966602 #1-505 Acq:31-OCT-1996 23:05:06 EI+ Voltage SIR 70T
445.7555 I>s3 Exp:EPCUS
TRIANGLE LABS Texts23A-2 TLHf39291Rl JKT. TIKE " 23:08
25 44
27s 00
24s 00
25s 00
26:00
27-00
4.7E4
3. 8E4
2.8E4
1.9E4
9.4E3
O.OEO
Time
.4.4E6
.3. 5E6
.2.6E6
.1. 8E6
.8.8E5
.O.OEO
Time
.9. OE6
.7.2E6
.5.4E6
.3. 6E6
.1. 8E6
.O.OEO
Tim,
.1. 8E7
.1. SE7
.1.1X7
.7.4E6
.3. 7E6
.O.OEO
Time
-------
ri!e:T9S6S02 #1-505 "M&ji31-oci!-19SG 33.-05.-gg EH- Voltage SttR 70"? NoiaesSSS
383.8156 Fs3 BSOS(2S6t30,-3.0) rKD(S,3,l,0.10%,2S16.0,0.00%,F,I') ExpiEPCOS
TRIANGLE LABS Texts23A-2 TLI#39291R1 HKT. TIME = 23:06
100* A2.72E5
24:36 24:48 25:00 25:12 25:24 25:36 25:48 26:00 26:12 26:24 26:36
Tile:T966602 #1-505 Acqs31-OCT-1996 23:05:06 EH- Voltage SIS 70T Nbise:1020
391.8127 F:3 BSUB(256, 30,-3.0) PXS(5,3,1, 0,101,4080.0, 0,00%, F,f) ExpiEPCOS
TRIANGLE LABS Texts23A-2 TLI#39291S1 JKT. TIKE - 23:08
100% A2.00E5
26:48
24:36 24:48 2SsOO 25:12 25:24 25:36 25:48 26:00 26:12 26:24 26:36
file:T966602 f 1-505 Acg:31-OCT-1996 23:05:06 EH- Voltage SIS 70T Noise:893
401.8558 F:3 BSUB(256, 30, -3. 0) PKD(5, 3,1, 0.10\, 3572.0,0.00\,F,F) Erp:EPCUS
TRIANGLE LABS Text:23A-2 TLI#39291R1 IWJ. TIME = 23:08
100* A2.28E7
Al.57E7
40.
201
26:48
.O.OES
Time
6.9KS
15.6BS
"-4.2E6
'.2.8X6
.1,4X6
o.oso
24:36 24:48 25:00 25:12 25:24 25:36 25:48 26:00 26:12 26-24
File:T966602 #1-505 Acg:31-OCT-1996 23:05:06 EI+ Voltage SIS 70T NoiseiB13
403.8529 F:3 BSBB(256, 30,-3 ,0 ) PKD(5, 3,1, 0 .10%, 3252. 0, 0. 00%, T, F) Exp:EPCas
TRIANGLE LABS Teits23A-2 TLI039291K1 JMT. TIME = 23:08
IOCS A1.83E7
A1.32E7
26:36 26:48
401
201
".4. 5E6
'-3.3E6-
"-2.2E6
11. ise
24:36 24:48 25:00 25:12 25:24 25:36 25:48 26:00 26:12
FileiT966602 #1-505 Acqs31-OCT-1996 23:05:06 EH- Voltage SIS 70T
392.9760 W:3 ExptEPCUS
TRIANGLE LABS Texts 33A-2 TLI#39291K1 IJKT, TIME
* "
so:
60-
40.
20:
0.
26:24 26:36
.0. OEO
Time
_1,8E7
~-i.se?
11.XE7
L7.4S6
L J. 7S6
24:36 24:48 25tOO 25:12 25:24 25:36 25:48 26:00 26:12 26:24 26:36 26:48
O.OEO
. Time
i- 4
-------
±le:T966602 #1-443 Acq:31-OCT-1396 23:05:06 £1+ Voltage SIS JOT m>iae:666
07.7818 F:4 SSUS(2S6,30r-3.0) PKD(5,3,1,0.10^,2664.0,0,00\,r,f) Eip:EPCUS
TSIAKGLE LASS Text:23A-2 TLI#39291X1 JWJ. TIKE - 23i08
00* A8.J.3E5
aol
28:12 28:24 28:36 28:48 29:00 29:12 29:24 29:36
F±letT966602 #1-443 Acq:31-OCT-1996 23:05:06 EI+ Voltage SIR 70T Woise.-S.21
09.7789 F:4 BSm(256,30,-3.0) PKS(5r3,l,0.10%,2484.0,Q.OO\,F,F) ExpiEPCUS
TRIANGLE LASS Text:23A-2 TLI#39291M1 I«T. TIME = 23:08
IOCS A7.47E5
80l
28:12 28:24 28:36 28:46 29:00 29:12 29:24 29:36
File:T966602 tl-443 Acq:31-OCT-1996 23:05:06 EI+ Voltage SIS 70T Noiae-,1264
417.8253 F:4 BSUS(256,30, -3.0) PKD(5,3,1, 0.10%,5056. 0, 0. 00%,F, F) ExpiEPCUS
TRIANGLE LABS Teit:23A-2 TLIK392S1R1 XJBT. TIME - 23:08
1001 A1.05E7
40
20:.
oj
A2.72E5
A/V
A1.45ES
/v
-2.6ES
.2.1E5
1.6E5
11. OE5
-5.2E4
29:48
30:00
O.OEO
X±me
60:
401
201
ol
A2.37E5
A1.45E5
yy.
2.5E5
"-.2.0E5
•.1.5E5
Ll. OE5
-5.0E4
29:48
30s 00
10. OEO
rime
ao;
sol
20:.
A5.14ES
3.3E6
12. 6JE6
-2.0E6
Ll. 3E6
'.6.SE5
28:12 28:24 28:36 28:48 29:00 29:12 29:24 29:36
Fil
-------
F±le:T3"6'6SWl2 "H-4"f3 Acq:lJl-OCT-199& 23:35:06 SX± Voltage Six 70T
423,7766 Fi4 BSUS(256,30, -3 .0} Pm>(S,3,l,0.1Q*,1968,OrO.QO*,F,F}
TRIANGLE LABS Text:23A-2 TLI#39291X1 JKT.
100J
so;
so;
40;
20;
A3.40E5
h
A3 . 19E5 I \
A ! \
/ \ / \
/ \ / \
/ \ A9.55E3 I \_
/\ / ^-~-X"™S — ^*V r— -— r— «- -- S\ -—- !**~ — rtr
Noise; 4 92
ExpsEPCUS
TIME = 23:08
Al . 51E4
V f**\ -"^ ^/\— *~Hs^ ^— -— — *S,.^X .^-...--^....irn,,,.
^1.2E5
"-9.8E4
17.3E4
14.9JE4
12.4Z4
" 0 . OEO
28-30 ' 28:36 ' 28s42 ' 28:48 ' 28:54 ' 29:00 ' 29sOS ' 29:12 ' 29sis ' 29:24' ' 29:30 ' 29.-3S ' 29:42 Time
FilesT966602 §1-443 Acq:31-OCT-1996 23:05:06 EH- Voltage SIS 70T
425.7737 F:4 BSUB(256,30, -3.0) P1O3(5,3,1, 0.10%,1844.0, 0.00%,f ,F)
TRIANGLE LABS Text:23A-3 TLI #39291X1 XKT.
1003
so;
eo;
40;
201
A3 . 74E5
A3 . 62E5 h
A i\
M / \
/ \ /I
/ \ \
^^ N — v _ ^ _ /\ __ __/ ^
'28-36 ' 28; iff ' 28:42 ' 28s 48 ' '28:54 ' '29:00 ' 29:06 ' 291-12 ' 29-
FilesT966602 #1-443 Ac?:31-OCT-1996 23:05:06 EH- Voltage SIR 70T
435.8169 F:4 BSUB(256, 30, -3 . 0) PKD(5, 3,1, 0.10%, 4504. 0, 0. 001, F,F)
TRIANGLE LABS Text:23A-2 TLI#39291R1 IKT.
1003
801
601
401
201
0"
Al -J2E7
A
\
y v
281-30 ' 281-36 ' '28:42 ' 28-48 ' 28«54 ' 29iOO ' 29:06 ' 29:12 ' 29:
rile.-T966602 #1-443 Acq:31-OCT-1996 23:05:06 EI+ Voltage SIR 70T
437.8140 Fs4 BSUB(256, 30, -3 . 0) JPKDf 5, 3,1, 0.10%,3340. 0,0 . 00%, FfF)
TRIANGLE LABS Text:23A-2 TX,I#39291R1 IJUT.
1003
BO;
eo;
40;
20.
0
Al . 66E7
r\
A
\
1 V
'28:30 ' 28; iff ' 28s42 ' '28:48 ' 28:54 ' 29:00 ' 291-06 ' 29:12 ' 29:
File:T96S602 #1-443 Ae?.-31-OCT-1996 23s05:06 EH- Voltage SIR 7QT
430.9729 Fs4 ExpsSPCOS
TRIANGLE LABS Text.-23.A-2 TLI #39291 XI JWJ.
100J
80.
60.
40.
20,
0
28:3328:38 28:43 28:59 29:06 -,0 11 ^JL1
28:30 281-36 '28:42 28:48 ' 28:54 ' *29;00 29s 06 ' 29:12 ' 29:
Noise: 4 51
ExpiEPCUS
TIMS - 23:08
-1 . 3E5
\ — ^ ^— V .— ^ J>
11 . OE5
'-7.6E4
15 . OE4
12 . 5E4
~ 0 . OEO
IB ' 29s 24 ' 29.-30 ' 29:36 ' 29:42 Time
Noise -.1126
ExpsEPCUS
TIME = 23:08
_5.6£6
14.5E6
13.3£6
12.2S6
11 . 1E6
" 0 . OEO
18 ' 29:24' ' 291-30 ' 29:36 ' 29s 42 Time
Noise: 835
ExpsEPCUS
TIME « 23 i 08
r5.4ES
14.3J5T6
13.2£6
12.1IT6
11.1E6
' 0 . OBO
18 ' 29:24 ' 29:30 ' 29:36 ' 29:42 Time
TIME - 23:08
7___^__^^^ 29:31 29:39
\-^/ ^-w^ xX™
1 . 3E7
11 . 0£7
17.5X6
15 . OE6
12.5BS
" 0 . 0^0
18 ' '29:24 ' 29.-30 ' 29s36 ' 29s42 Time
-------
File:T366602 fl-443 Acqi31-OCT-1996 23:05:06 EI+ Voltage SIS 70T MbxaesSSg
441.7428 F:4 BSUB(256,30, -3.0) PKD( 7,2,3, 0.10\,3556. 0,0. QQ%,T,F) ExptEPCnS
TRIANGLE LASS Texts 23A-2 HI #39291X1 IKJ. TIME - 23:08
1003
901
801
701
601
501
401
30\
20;
101
Al.
j^ ^ j^
7E6
v^ . ^ . ^
'29:00' ' ' ' '30!0o' ' ' ' '31:00' ' ' ' 33\00 ' ' '33:00
File:T966602 fl-443 Acq:31-OCT-1996 23:05:06 EI+ Voltage SIS 70T Noiae:772
443.7399 F:4 BSUB(256,30,-3.0) FKD(7,2,3, 0.10\,3088. 0,O.QQ\,F, F) Exp:EPCUS
TSIAHSLE LASS Text:23A-2 TLI#39291S1 IJKT. TIME - 23s 08
1003
901
SOI
701
601
501
401
301
201
101
Al.
L_» *-« . _AA* *.-
8E6
\_ , .
'29:00 30s 00 ' ' ' ' 31s 00' ' ' ' '32:00 33:0o'
File:T9666Q2 fl-443 Acq:31-OCT-1996 23:05:06 EI+ Voltage SIS TOT
430.9729 Fi4 ExpiEPCUS
TRIANGLE LABS Text:23A-2 TLI#39291X1 IKJ". TIME " 23:03
10v]& __ ^_ on . j >? 5O«fiT^ yn. vy 30:59 31. 07 «. .. .»« ~ *
901
801
701
60-
501
401
301
20.
10,
OJ
28:43 **ij.' in -•>».->.« i A 3-L:fa j^:^* 33-01
(Vf^MW^^ /%V/^rAAAA/wMAAA 33,2*
1 vv-y^ w yv \r/»vi»yui'U A/
V
29:00 30:00' ' ' '3li-00 32:00 ' 33:00
File:T966602 #1-443 Acq:31-OCT-1996 23:05:06 EH- Voltage SIB 70T
513.6775 r:4 ExpsEPCUS
TRIANGLE LASS Teuct:23A-2 TLI&39291R1 IJET. TIME - 23:08
1003
90,
80.
70.
60.
50.
40.
30.
20.
10.
0.
33
32:27
30 . (8 31s 12 31:50
i i I lit
11 I' ,J 'TI/Tlfla iT* 1 , ill i «•«
jy^Mii^^
29:00 30:00 31:00 32s 00 33:00
-3.8JE5
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.3.1E5
.2.7E5
-2.3ES
_1 . 9E5
•-1.5E5
-.1.2E5
'-.7.7E4
-.3 , 8£4
: 0 . OEO
Time
-4.1ES
-3.7E5
\3,3E5
L2.BE5
1.2 . 4E5
~L2.QE5
Ll . 6E5
L1.2E5
:.8.1E4
14.1E4
Time
,.1.327
^A
1
'.
L1.2E7
11 . OE7
L9.2ES
17.9E6
L6.6ES
L5.2E6
13 . 9E6
L2.6E6
''•.1.3X6
'• 0 . OEO
Time
34 1.4E4
rt/i
-1.3E4
.1.1E4
-9.9E3
.8.5E3
'.7.1E3
.5.SE3
'•.4.2E3
':2.m3
Ll . 4E3
: 0 . OEO
Tiae
-------
*Het'T966602 il-443 Acqs31-OCf~19$6 23:05:
457.7377 F:4 BS ExpsEPCVS
IKT. TIME - 23:08
31:54 32:00 32:06 ' ' ' 32*1J
06 EJ* Voltage SIR 701 Noise: 4 34
,10%,1736.0,0.00%,r,F^ EXpiEPCVS
IJKT. TIME - 23:08
31:54 ' ' ' 32*00 ' ' ' 32:06 ' ' ' 32:12
06 £1+ Voltage SIS 70T No±ae:200
,10%,800.0,0,00%,1',F; Erp.-EPCGS
JWT. TIME = 23 : 08
31*36 ' ' ' 31*42 ' ' ' 31:48 ' ' ' 31*54 ' ' ' 32.-00 ' ' ' ~32\06 ' ' ' 32:12
ST966602 #1-443 Acg:31-OCT-15S6 23:05:06 EJ* Voltage SIS 70T Noise:229
7750 F:4 BSUS{256, 30, -3.0) PXJ)(7, 2, 3, 0.101,916 .0,0. 00%, F,F) Elp:EPCUS
NGX.E LABS Text:23A-2 TZI#39291S1 JKT. TIME = 23s 08
A2.71E7
A
/ \
/ \
J V
; i j i i ) » 1 i > t 1 • 1 ! 1
31:36 31.-42 31.-48
iTS66602 #1-443 acg:31-OCT-!SS6 23:05:
S725 F:4 Exp:EfCVS
iNGLE LABS Tejct:23A-2 TLI#39291R1
31*36 31:42 ' ' 31:48
31*54 ' ' ' 32.-00 ' ' ' 32.-06 ' ' ' 32*li
06 EI+ Voltage SIS 70T' •
INJ". TIME = 23:08
31:54 32:00 32:06 ' ' ' 32.Lli
.3.1*5.
12.5E5
-1.9X5
11 . 3E5
16.3E4
"O.OEO
Time
_3 . 6E5
12.SE5
12.2E5
11.5E5
17.3E4
" 0 . OEO
Time
16.2E6
14.6E6
13.1E6
11 . 5E6
'O.OEO
Ziffle
-S.3E6
17.5E6
15.6E6
.3 . 7E6
11.SE6
O.OEO
1 Tiae
1.2E7
-5.5E6
-7.5E6
15.0E6
-2.5E6
' 0 . OEO
Time
1- 3
-------
fitf, lass 2£.&5 Peak top
Htight 5.81 volts Span 288 ppi
Sustei file
Data File
issdution
Group nuibir
a £83
8 384
C 386
0 31S
E 318
F 328
3 32!
L 334
PI 348
N 3€
0 352
P 354
9 358
8
;58
EPCUS
ft'TIB3196
I
fef, masses £32.125, 416,37
T m
U 3/6
V 410
ChmeL I '32i,378E Peak top
Httght 4,45'JOlts Span 268 opt
1 9
-------
File:T966602 #1-835 Acq:31-OCT-199~6 23:05:06 EH- Voltage SIR 70T Noise:1769
303.9016 F:2 BSUB(256,30,-3.0) PKD(7,3,1,0.10%,7076.0,0.00%,F,T) Exp:EPCUS
Sample Text:23A-2 TLI#39291R1 IHL_TIME = 23:08 File Text:23A-2 TLI#39»
lOOi, (K.8. jJOl?} ^AeTliil^ A7.05E4 _2.7E4
50:
.1.4E4
Time
File:T966602 #1-835 Acq:31-OCT-1996 23:05:06 EI+ Voltage SIR 70T Noise:1333
305,8987 F:2 BSUB(256,30,-3.0) PKD(7,3,1,0.10%,5332.0,0.00%,F,T) ExprEPCUS
Sample Text:23A-2 TLI#39291R1 INJ. TIME = 23:08 File Text:23A-2 TLI#39»
100* (Si. 66E5J) r_5.0E4
50J
0
A8.80E4
i—i—I—i—i—i—i—r
T 1 1 1 1 1 1 1 1 1 1 r—T r-—i 1——i r—I r—[ 1 1 1 1 1 1 1 1 1 1 1 r
13:06 13:12 13:18 13:24 13:30 13:36
.,—,—,—,—i—,
12.5E4
O.OEO
13:42
Time
12:54 13:00
File:T966602 #1-835 Acq:31-OCT-1996 23:05:06 El-f Voltage SIR 70T
315.9419 F:2 Exp:EPCUS
Sample Text:23A~2 TLI#39291R1 INJ. TIME = 23:08 File Text:23A-2 TLI#39»
13^37 r!.2E4
13:34
50_:
12:55
-i—i—i—i—i—i—r-
!—~p—i r~*~i i i 1 1 1 1—i 1 1 ? 1 1 1—i i 1 1 1 1—"T 1 1 1 1™
13:12 13:18 13:24 13:30 13:36 13i42
16.1E3
.O.OEO
Time
12:54 13:00 13:06
File:T966602 #1-835 Acq:31-OCT-1996 23:05:06 EI+ Voltage SIR 70T
317.9389 F:2 Exp:EPCUS
Sample Text:23A-2 TLI#39291R1 INJ. TIME = 23:08 File Text:23A-2 TLI#39»
100%. 13; 18 _1.1E4
13:03
SOJ
13:36
12:54
T - 1 - 1 - 1 - 1 - 1 - 1 - 1
1
12:54 13:00
13:06
13 :
13:18 13:24 13:30 13:36
_,——,_
13:42
15.4E3
O.OEO
Time
-------
?ile:T966602 #1-835 Acq: 31-OCT-1996 23:05:06 EI+ Voltage SIR 70T Noise:1769
503.9016 F:2 BSUB (256 , 30, -3 . 0) PKD(7, 3 , 1, 0 . 10%, 7076 . 0, 0 . 00%, F,T) Exp:EPCUS
Sample Text:23A-2 TLI#3929lRl INJ. TIME = 23:08 File Text:23A-2 TLI#39»
100%, A1.94E5 ' -- -- ~~^ ,_4.3E4
A2.87E5
A8.25E4
50J
2.2E4
1 — i — i — i — i — i — I — i — r~r — i — i — I — i — i — r~t — r—j — i — i — i — i — i — | — i — i — i — i — i — | — i — i — i — i — i — i — i — i — i — i — i— i
14:12 14:18 14:24 14:30 14:36 14:42 14:48 14:54 15:00 15:06 15:12 15:18 15:24 15:30 Time
?ile:T966602 #1-835 Acq: 31-OCT-1996 23:05:06 EI+ Voltage SIR 70T Noise: 1333
JOS. 8987 F:2 BSUB (256, 30, -3 . 0} PKD(7, 3 , 1, 0 . 10%, 5332 . 0, 0 . 00%, F,T) Exp:EPCUS
Sample Text:23A-2 TLI#39291R1 INJ. TIME = 23:08 File Text:23A-2 TLI#39»
100%, -., --- - -- _
CA3.64_E|>
A5.06E4
Vi i—i i i i i i i—i—i—i—i—i—i—i—i—i—i—i—i—i—i—i—i—i—i—i—i—i ii—i—i—i—i—i—i—i—i—i—i—i—i—i—i—n—i—i—i—i—i—i—i—i—i—i—i—i—i—i—i—i—i—i—i i < i i—i—i—i—i—i i i—i—i—
14:12 14:18 14:24 14:30 14:36 14:42 14:48 14:54 15:00 15:06 15:12 15:18 15:24 15:30 Time
?ile:T966602 #1-835 Acq:31-OCT-1996 23:05:06 EI+ Voltage SIR 70T
315.9419 F:2 Exp:EPCUS
Sample Text:23A-2 TLI#3929lRl INJ. TIME = 23:08 File Text:23A-2 TLI#39»
100% _4.8E5
0.
14:38
12.4E5
OEO
14:12 14:18 14:24 14:30 14:36 14:42 14:48 14:54 15:00 15:06 15:12 15:18 15:24 15:30 Time
File:T966602 #1-835 Acq: 31-OCT-1996 23:05:06 EI+ Voltage SIR 70T
317.9389 F:2 Exp:EPCUS
Sample Text:23A-2 TLI#3929lRl INJ, TIME = 23:08 File Text:23A-2 TLI#39»
1004 _6.4E5
50J
0
14:38
15:10
13.2E5
O.OEO
14:12 14:18 14:24 14:30 14:36 14:42 14:48 14:54 15:00 15:06 15:12 15:18 15:24 15:30 Time
-------
?ile:T966602 #1-835 Acq:31-OCT~1996 23:05:06 EI+ Voltage SIR 70T Noise:1769
303.9016 F:2 BSUB(256, 30, -3 . 0) PKD(7, 3, 1, 0.10%, 7076.0, 0 .00%, F,T) Exp:EPCUS
Sample Text:23A-2 TLIJ3JJ2 9.1R1 INJ. TIME = 23:08 File Text:23A-2 TLI#39»
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File:T966602 #1-835 Acq:31-OCT-1996 23:05:06 EI+ Voltage SIR 70T Noise:1333
305.8987 F:2 BSUB(256,30,-3.0} PKD(7,3,1,0 .10%,5332.0,0.00%,F,T) Exp:EPCUS
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File:T966602 #1-835 Acq:31-OCT-1996 23:05:06 EI+ Voltage SIR 70T
315.9419 F:2 Exp:EPCUS
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File:T966602 #1-835 Acq:31-OCT-1996 23:05:06 EH- Voltage SIR 70T
317.9389 F:2 Exp:EPCUS
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305.8987 F:2 BSUB(256,30,-3 .0) PKD(7,3,1, 0.10%,5332.0,0.00%,F,T) Exp:EPCUS
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319.8965 F:2 BSUB(256,30,-3.0) PKD(7,3,1,0.10%,4136.0,0.00%,F,T) Exp:EPCUS
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321.8936 F:2 BSUB(256,30,-3.0) PKD(7,3,1,0.10%,2332.0,0.00%,F,T) Exp:EPCUS
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File:T966602 #1-835 Acq:31-OCT-1996 23:05:06 EI+ Voltage SIR 70T
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V
-------
TLI Project: 39291rl
Client Sample: 23A-2
Method 23 TCDD/TCDF Analysis (DB-225)
Analysis File: X964234
Client Project:
Sample Matrix:
TLI ID:
Eastern Ridge Lime Facility
M23TRAIN Date Received: 10/19/96
143-23-2A/B Date Extracted: 10/21/96
Date Analyzed: 11/01/96
Spike File: SPC2NF08
ICal: XF21266
ConCal: X964226
Sample Size:
Dry Weight:
GC Column:
1.000
n/a
DB-225
Dilution Factor: n/a
Blank File: T966616
Analyst: JF
% Moisture: n/a
% Lipid: n/a
% Solids: n/a
2,3,7,8-TCDF
0.02
0,77
20:22
13C,2-2,3,7,8-TCDF
6,0
75,1
40%-130%
0,79
20:22
13C,2-1,2,3,4-TCDD
0.80
19:24
Data Reviewer I^^J-jjt^T
Page 1 of 1
11/11/96
C2NF_PSR vl.14, LARS 6.08.00
Triangle Laboratories, Inc.®
801 Capitals Drive • Durham, North Carolina 27713
Phone: (919) 544-5729 • Fax: (919) 544-5491
Printed: 16:1211/11/96
121
-------
Data Review By:
Initial ....Date...
jLL/_£L/Jfe Calculated Noise Area:
7.00
The Total Area for each peak with an ion abundance ratio outside
ratio limits has been recalculated according to method requirements.
Page No.
11/01/96
Listing of X964234B.dbf
Matched GC Peaks / Ratio / Ret. Time
Compound/
M_Z.... QC.Log Omit Why ..RT. OK Ratio Total.Area. .. Area.Peak.1.. Area.Peak.2.. Rel.RT Compound.Name.. ID.
TCDF
304-306 DC NL
DC SN
DC SN
DC SN
DC SN
DC SN
DC SN
DC SN
DC SN
DC SN
DC SN
DC SN
304-306 21
13C12-TCDF
316-318 DC NL
DC WL
DC WL
DC WH
316-318 2
0:00
16:10
16:18
16:23
16:48
16:53
17:08
17:14
17:30
17:40
17:48
17:55
18:01
18:13
18:20
18:42
19:07
19:11
19:22
19:32
19:43
19:53
20:01
20:15
20:22
20:33
20:43
20:52
21:29
21:36
21:44
21:48
22:07
Peaks
0:00
19:05
19:21
20:22
20:52
22:09
Peaks
0.
RO
RO
RO
RO
RO
RO
RO
RO
RO
RO
RO
RO
RO
RO
RO
RO
RO
RO
RO
RO
RO
RO
RO
0.
RO
RO
RO
RO
65-0.89
0.27
1.37
3.93
2.53
0.65
0.49
1.02
0.60
0.97
0.24
1.05
0.36
1.13
0.74
1.19
0.75
0.80
1.49
0.78
1.00
0.58
0.93
0.69
0.77
0.77
0.78
0.70
1.03
1.23
0.31
1.96
1.09
0.27
,65-0.89 •
3.76
0.54
0.90
0.79
0.78
0.62
0.788-1.094
3,
59.
2.
0.
5,
3.
49.
62
37.
2
48
52
28
145
38
185
47
11
83
44
20
54
7
46
57
64
40
45
17
3
2
4
2
1,230
1
42
137
24,293
248
274
24,541
.54
,69
,69
.97
,62
.61
.03
.19
.04
.07
.50
.97
.69
.72
.96
.87
.11
.52
.33
.26
.27
.88
.22
.40
.86
.56
.14
.29
.88
.81
.23
.15
.35
.64
.54
.53
.94
.10
.12
.08
.22
46.
28,
26
20
28
23
18
62
26
79
21
36
24
8
28
20
25
28
16
26
12
10,704
109
.25
.32
.95
.33
.81
.19
.32
.17
.17
.57
.00
.48
.99
.84
.78
.19
.09
.23
.48
.32
.41
.00
.00
33.
27
45
20
27
63
16
83
22
106
26
46
25
15
31
26
32
36
23
25
10
13,589
139
.68
.64
.20
.90
.36
.86
.21
.55
.04
.30
.11
.85
.02
.18
.06
.21
.77
.33
.66
.62
.12
0.
.10
.12
0
0.
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
1
1
1
1
1
1
1
1
1
.000
.794
.800
.804
.825
.829
.841
.846
.859
.867
.874
.880
.885
.894
.900
.918
.939
.942
.951
.959
.968
.976
.983
.994
.000 2378-TCDF AN
.009
.017
.025
.055
.061
.067
.070
.086
951-1.049
0
0
0
1
1
1
.000
.937
.950
.000 13C12-2378-TCDF ISO
.025
.088
Triangle Laboratories, Inc.® Analytical Services Division
801 Capitola Drive • Durham, North Carolina 27713
Phone: (919) 544-5729 • Fax: (919) 544-5491
Printed: 17:5811/01/96
123
-------
Page No.
11/01/96
Listing of X964234B.dbf
Matched GC Peaks / Ratio / Ret. Time
Compound/
M_Z.... QC.Log Omit Why ..RT. OK Ratio Total.Area... Area.Peak.1.. Area.Peak.2.. Rel.RT Compound.Name.. ID..
13C12-TCDD
332-334
332-334
DC
DC
DC
DC
NL 0:00
18:11
19:13
19:24
20:05
WH 21:26
WH 21:37
WH 21:43
4 Peaks
0.
RO
RO
RO
RO
65-0.89
1.29
1.04
0.78
0.80
0.82
1.24
0.70
1.48
Above: TCDF / TCDD Follows
0.896-1.104
1.38 0.000
60.93 35.74 34.49 0.946
16,234.92 7,102.39 9,132.53 1.000 13C12-2378-TCDD IS1
11,660.55 5,180.75 6,479.80 1.010 13C12-1234-TCDD RSI
185.96 83.75 102.21 1.045
6.01 1.115
19.86 1.125
12.05 1.130
28,142.36
Column Description "Why" Code Description QC Log Desc.
M_Z -Nominal Ion Mass(es)
. .RT. -Retention Time (mnuss)
Rat.l -Ratio of M/M+2 Ions
OK -RO=Ratio Outside Limits
Rel.RT-Relative Retention Time
End of Report
WL-Below Retention Time Window
WH-Above Retention Time Window
SN-Below Signal to Noise Level
-------
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Sansplo Text:23A-2 TLI#39291rl fila Texts TRIANGLE LABS
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Time
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401
201
17:00 18:00 19:00 20:00 21:00
Fila:S964234 01-784 Acq: l-NOV-1996 17:28:42 OC El* Voltage SIR AvtoSpac J?oise:505
331.9368 BSUB(2S6,30,-3.0) PXD(5,3, 1, 0.10%,2020. 0, 0, OOX,F,F)
SarapJe T«xt:23A-2 Til#35251rl File TaxtiTRIANGLE LABS
1003B A7.JOB7
80.
601
401
201
17:00 18.-00 15:00
Fila:X964234 #1-784 Acq: l-KOV-1996 17:28:42 OC BI+ Voltage SIR AutoSpec ttoise:38B
333.9338 BSUB{256,30,-3.0) PKD(S,3, 1, 0,10%, 1552. 0,0.00%,F,J?j Exp:XCONF_TT
Sample Text:23A-2 TLX#39291rl Filt Text:TRIANGLE LABS
AS,J.3S7
80j \\L6.48E7
SOI
401
201
0.
7:00
18:00
15:00
.1.7E7
.1.4E7
.1. OE7
.7.0E6
.3. 5E6
.O.OEO
.1.4E7
.1.1X7
.B.3E6
.S.6E6
.2.8E6
.O.OEO
20:00
21:0o'
'.1.4E7
12.2JE7
17.IBS
13. SB*
.O.OEO
Tina
-------
File:X964234 #1-784 Acq: 1-SOV-19S6 17:28:42 OC EX+ Voltmgm SIS AutoSpec
303.9016 Exp:XC08F_TT
Staple Text:23A-2 TLI«3929H1 File Text : TRIANGLE UtBS
100%
•
80J
sol
401
201
•
0"
16
18 42
18*13
17*14 1
i it Ik I7«f3 r \ 19>a2 1S'53 2°133
lF|I 16,43 \]f* Ikd Ml |/y Uft 1 1 IU | lA H JM AA/l hAzi-O/1!'25 22tO<|
.1.7*5
.1.325
.9.9S4
.6.6E4
~3.3E4
O.OEO
00 17*00 18*00 15*00 20*00 21*00 22*00 Time
File:X964234 #1-784 Acq: l-NOV-1996 17:28:42 QC SI* Voltage SIR AutoSpac
315.9419 Exp:XCOHF_TT
Sas&lm Taxt:23A-2 TLI#39291ll File Text : TRIANGLE LABS
100*
801
601
401
201
0'
IS
20:22
"
.
/ V
-2.5S7
-2.0E7
-1.5E7
.1.0*7
.S.OE6
O.OEO
00 17*00 ' ' ' 18*00 ' ' ' 1.9*00 ' ' ' 20*00 ' ' ' 21*00 ' ' ' 22*00 ' ' Time
File:X964234 #1-784 Acq: l-NOV-1996 17:28:42 QC 21+ Voltaff* SIR AutoSpec
319.8965 Exp:XCONF_TT
Sasple Text:23A-2 TLI#39291rl File Text t TRIANOLS LABS
1003s
80J
601
401
201
'.
o-
16
17*00
17*31
i
1
\ 1 i a t n ^^ 1 25 21 * 51 1
Z$s3S j L / \ M, i A . *, Ar\A 20s07 .20s41 21:10 [ jft
[V»^vv«sAVw*«Aw^vj>'swy ^tA*£*J V\^\rfAMjk^" ^*«u*r N^U»jM^Jrfg»J^U^'Vw' *^\AAJUUJ*'^**'*^l'*MW^AN%A*^A^w-*^^ MvsM»
-------
Peak Locate Examination: l-NOV-1996:17:28 File:X964234
Experiment:XCONF_TT Function:1 Reference:PFK
-------
TLI Project: 39291x1
Client Sample: 23A-3
Method 23 PCDD/PCDF Analysis (a)
Analysis File: T966603
Client Project:
Sample Matrix:
TLI ID:
Sample Size:
Dry Weight:
GC Column:
Eastern Ridge
M23TRAIN
143-23-3A-C
1.000
n/a
DB-5
Lime Facility
Date Received:
Date Extracted:
Date Analyzed:
Dilution Factor:
Blank File:
Analyst:
10/19/96
10/21/96
10/31/96
n/a
T966616
BB
Spike File:
ICal:
ConCal:
% Moisture:
% Lipid:
% Solids:
SPX23708
TF53286
T966598
n/a
n/a
n/a
2,3,7,8-TCDD
1,2,3,7,8-PeCDD
1,2,3,4,7,8-HxCDD
1,2,3,6,7,8-HxCDD
1,2,3,7,8,9-HxCDD
1,2,3,4,6,7,8-HpCDD
1,2,3,4,6,7,8,9-QCDD
2,3,7,8-TCDF
1,2,3,7,8-PeCDF
2,3,4,7,8-PeCDF
1,2,3,4,7,8-HxCDF
1,2,3,6,7,8-HxCDF
2,3,4,6,7,8-HxCDF
1,2,3,7,8,9-HxCDF
1,2,3,4,6,7,8-HpCDF
1,2,3,4,7,8,9-HpCDF
1,2,3,4,6,7,8,9-OCDF
:-:-y.-:-:^vffi<-'<-y.<<
-------
TLI Project: 39291rl
Client Sample: 23A-3
Method 23 PCDD/PCDF Analysis (a)
Analysis File: T966603
13C,2-2,3,7,8-TCDF
>3C,2-2,3,7,8-TCDD
13Cl2-l,2,3,7,8-PeCDF
13C,2-l,2)3,7,8-PeCDD
13Ci2-l,2,3,6,7,8-HxCDF
13Ct2-l,2,3,6,7,8-HxCDD
13C12-l,2,3,4,6,7,8-HpCDF
»C,2-l,2,3,4,6,7,8-HpCDD
"C«-1,2>3,4)6,7,8>9-OCDD
6.3
6.6
6.1
5.6
6.5
7.3
7.1
7.1
12.9
78.4
82.4
75.7
70.2
81.4
90.8
89.1
89.1
80,7
40%-130%
40%-130%
40%-130%
40%-130%
4Q%-130%
40%-130%
25%-130%
25%-13Q%
25%-130%
0.74
0.78
1.52
1.49
0.48
1.23
0.42
1.05
0.84
15:36
16:23
20:51
22:18
25:20
26:10
28:18
29:14
31:42
37CLr2,3,7,8-TCDD
13C,2-2,3,4,7,8-PeCDF
l3Ci2-l,2,3,4,7,8-HxCDF
I3Ci2-l,2,3,4,7,8-HxCDD
13C,2-l,2,3,4,7,8,9-HpCDF
4.3
4.3
4.7
4.3
4.7
107
107
117
108
117
70%-140%
70%-140%
70%-140%
70%-140%
70%-140%
1.47
0.48
1.25
0.43
16:24
21:51
25:13
26:05
29:34
l3Ci2-l,2,3,7,8,9-HxCDF
13Ci2-2,3,4,6,7,8-HxCDF
4.1
4.0
103
100
40%-130%
40%-130%
0.47
0.49
26:41
25:55
^^SS!^S^A^l^:^:^
13C12-1,2,3,4-TCDD
'3Ci2-l,2,3,7,8,9-HxCDD
0.81
1.24
16:09
26:29
Data Reviewer
11/11/96
Page 2 of2
X237.PSR »U4, LASS 6,08,00
Triangle Laboratories, Inc.®
801 Capitola Drive » Durham, North Carolina 27713
Phone: (919) 544-5729 • Fax: (919) 544-5491
Printed: 16:04 11/11/96
13G
-------
TLI Project: 39291rl
Client Sample: 23A-3
Toxicity Equivalents Report
Analysis File: T966603
Client Project:
Sample Matrix:
TLI ID:
Sample Size:
Dry Weight:
GC Column:
Eastern Ridge Lime Facility
M23TRAIN Date Received: 10/19/96
143-23-3A-C Date Extracted: 10/21/96
Date Analyzed: 10/31/96
1.000 Dilution Factor: n/a
n/a Blank File: T966616
DB-5 Analyst: BB
Spike File:
ICal;
ConCal:
% Moisture:
% Lipid:
% Solids:
SPX23708
TF53286
T966598
n/a
n/a
n/a
2,3,7,8-TCDD
1,2,3,7,8-PeCDD
1,2,3,4,7,8-HxCDD
1,2,3,6,7,8-HxCDD
1,2,3,7,8,9-HxCDD
1,2,3,4,6,7,8-HpCDD
1,2,3,4,6,7,8,9-OCDD
TOTAL PCDD
2,3,7,8-TCDF
1,2,3,7,8-PeCDF
2,3,4,7,8-PeCDF
1,2,3,4,7,8-HxCDF
1,2,3,6,7,8-HxCDF
2,3,4,6,7,8-HxCDF
1,2,3,7,8,9-HxCDF
1,2,3,4,6,7,8-HpCDF
1,2,3,4,7,8,9-HpCDF
1,2,3,4,6,7,8,9-OCDF
TOTAL PCDF
0.01
0.02
0.02
0.02
0.02
0.03
0.13
0.03
0.01
0.02
0.02
0.01
0.01
0.02
0.02
0.02
0.03
x
X
X
X
X
X
X
X
X
X
X
X
X
X
X
X
X
1
0.5
0.1
0.1
0.1
0.01
0.001
0.1
0.05
0.5
0.1
0.1
0.1
0.1
0.01
0.01
0.001
0.01
0.01
0.002
0.002
0.002
0.0003
0.00013
0.0264
0.003
0.0005
0.01
0.002
0.001
0.001
0.002
0.0002
0.0002
0.00003
0.0199
Total EPA TEFs, 1989a: 0.0464 ng
Page 1 of 1
TEFPR vj.08, LARS 6.06.00
Triangle Laboratories, Inc.®
801 Capttola Drive • Durham, North Carolina 27713
Phone: (919) 544-5729 • Fax: (919) 544-5491
Printed: 16:21 11/11/96
-------
Data Review By:
Initial. Date...
I ' / ' I/ Vfe Calculated Noise Area:
3.'92
The Total Area tor each peak with an ion abundance ratio outside
ratio limits has been recalculated according to method requirements.
Page No.
11/11/96
Listing of T966603B.db£
Matched GC Peaks / Ratio / Ret. Time
Compound/
M_Z.... QC.Log Omit Why ..RT, OK Ratio Total.Area,.. Area.Peak.1.. Area.Peak.2.. Rel.RT Compound,Name.. ID.
TCDF
304-306
M
M
M
A
304-306
13C12-TCDF
316-318
316-318
TCDD
320-322
M
A
A
M
D
D
DC NL 0 : 00
13:05
13:24
13:36
13:51
14:04
14:20
14:25
14:39
14:53
15:00
15:11
15:25
15:37
16:03
16:19
15 Peaks
DC NL 0 : 00
14:38
15:11
15:36
16:04
4 Peaks
DC NL 0 : 00
14:02
14:20
14:34
15:10
15:26
DC SN 15:37
15:51
16:09
16:17
D SN 16:24
D SN 16:36
DC SN 16:39
DC SN 17:40
0.65-0.89
RO 0.96
0.86
0.78
0.69
0.81
0.82
0.73
0.82
0.86
0.72
0.87
0.79
RO 1.00
0.80
0.89
0.87
1
0.65-0.89
0.71
0.77
0.75
0.74 7
0.78
7
0.65-0.89
RO 1 . 04
0.77
0.77
0.75
0.82
RO 1.10
RO 1.51
0.74
RO 0 . 62
RO 0.61
RO 0.33
RO 0.30
RO 1.60
RO 2.70
0.828-1.138
6.89
88.76
48.71
37.73
229.12
154.96
51.61
54.43
96.30
79.46
69.43
36.20
36.82
127.04
31.80
20.61
,162.98
40.95
21.40
15.38
102.74
69.98
21.76
24.47
44.60
33.22
32.25
15.93
20.90
56.40
15.00
9.61
47.81
27.31
22.35
126.38
84.98
29.85
29.96
51,70
46.24
37.18
20.27
20.80
70.64
16.80
11.00
0.000
0,839
0.859
0.872
0.888
0.902
0.919
0.924
0.939
0.954 '
0.962
0.973
0.988
1.001 2378-TCDF AN
1.029
1.046
0.936-1.064
4.21
48.05
20.91
,193.50
57.18
,319.64
TYTM7 / rpy"i
IVi/r / iv
2.94
238.60
117.85
6.86
65.12
15.77
1.73
13.14
15.49
28.96
3. 75
2.92
0.62
0.48
20.88
8.99
3,052.84
25.09
104.05
51.41
2.93
29.37
9.78
5.60
6.74
12.60
27.17
11.92
4,140,66
32.09
0.
134.55
66.44
3.93
35.75
8.91
7.54
10.90
20.50
0.000
0.938
0.973
1.000 13C12-2378-TCDF ISO
1.030
846-1.086
0.000
0.857
0.875
0.889
0.926
0.942
0.953
0.967
0.986
0.994
1.001 2378-TCDD AN
1.013
1.016
1.078
Triangle Laboratories, Inc.® Analytical Services Division
801 Capitola Drive • Durham, North Carolina 27713
Phone: (919) 544-5729 • Fax: (919) 544-5491
Printed: 15:52 11/11/9§ 3 3
-------
Page No.
11/11/96
Listing of T9666Q3B.dbf
Matched GC Peaks / Ratio / Ret. Time
Compound/
M_Z.... QC.Log Omit Why ..RT. OK Ratio Total.Area... Area.Peak.1.. Area.Peak.2.. Rel.KT Compound,Name.. ID..
320-322
37C1-TCDD
328
328
13C12-TCDD
332-334
332-334
PeCDF
340-342
D
D
340-342
13C12-PeCDF
352-354
8 Peaks
501.79
0.878-1.122
352-354
DC
DC
DC
DC
DC
DC
DC
DC
D
D
DC
DC
DC
NL 0 : 00
14:57
SN 16:02
16:24
2 Peaks.
0.
NL 0:00 RO
15:11
BD 16:09
16:23
16:47
4 Peaks
NL 0 : 00
18:00
SN 19:13
SN 19:21
19:29
19:41
19:56
20:27
SN 20:35
20:47
20:53
21:05
21:10
SN 21:18
21:51
SN 22:01
SN 22:21
SN 23:00
SN 23:04
10 Peaks
NL 0 : 00
19:39
20:24
20:51
21:15
21:51
22;58
6 Peaks
RO
1.
RO
RO
RO
RO
RO
RO
3,
3,
65-0.89
2.92
1.
0.
0.
0.
14
81 3,
78 6,
82
9,
32-1.78
0.
1.
0.
0.
1.
1.
1.
1.
1,
1.
1.
52
54
64
28
56
58
53
.46
.42
,39
,58
2.41
2.34
9.74
1.69
RO
RO
RO
1
RO
RO
RO
RO
3.16
1
0
1
.31
.80
.72
1.05
58.65
1.15
118.52
177.17
3.33
22.34
621.60
263.21
68.41
975.56
«__._ ,
JLL.ULJ /
1.63
49.87
0.56
0.55
18.06
.76.82
16.98
36.40
1.60
14.77
13.23
5.97
1,35
1.58
16.02
6.78
4.00
1.12
0.79
249.47
58.
3,118.
65
52
14.40
1,615.
.55
2,751.04
30.75
0.000
0.913
0.979
1.001 37C1-TCDD S0R1
0.878-1.122
0.000
12.62
2,006.
3 , 512 .
37.
05
,17
,66
0.927
0.986 13C12-1234-TCDD
1.000 13C12-2378-TCDD
1.024
RSI
IS1
30.
11
47
10
21
8
8
5
1
10
,23
.00
.07
.27
.60
.59
.10
.64
.24
.07
19.
7
29
6
14
6
5
2
0
5
.32-1.78
0
3
1
1
1
1
1
.48
.42
.00
.52 6
.31
.47 3
.57
10
0.68
12.44
13.92
,621.01
27.32
,600.87
8.17
,283.73
16
8
3,989
16
2,145
4
.69
.46
.36
.60
.68
.99 '
4
8
2,631
12
1,455
3
0.855-1.112
.64
.06
.75
.71
.80
.18
.13
.34
.53
.95
0.
.88
.46
.65
.68
.19
.18
0.000
0.863
0.922
0.928
0.934
0.944
0.956
0.981
0.987
0.997
1.002 12378-PeCDF
1.011
1.015
1.022
1.048 23478-PeCDF
1.056
1.072
1.103
1.106
808-1.192
0.000
0.942
0.978
1.000 13C12 -PeCDF 123
1.019
1.048 13C12 -PeCDF 234
1.102
AN
AN
IS2
SUR
Triangle Laboratories, Inc.® Analytical Services Division
801 Captola Drive • Durham, North Carolina 27713
Phone: (919) 544-5729 • Fax: (919) 544-5491
Printed: 15:52 11/11/96
133
-------
Page No.
11/11/96
Listing of T966603B.dbf
Matched GC Peaks / Ratio / Set. Time
Compound/
M_Z OC.Log Omit Why ..RT. OK Ratio Total.Area... Area.Peak.1.. Area.Peak.2.. Rel.RT Compound.Name.. ID..
PeCDD
356-358
DC
DC
DC
DC
NL
SN
SN
SN
0
19
20
20
20
20
:00
:55
:23
s32
:39
:56
1.
RO
RO
RO
RO
21:21
D
D
356-358
13C12 -PeCDD
368-370
368-370
DC
DC
DC
D
DC
DC
DC
D
DC
DC
DC
SN
SN
SN
SN
SN
SN
SN
SN
WH
WH
4
NL
3
21
21
22
22
22
22
22
22
22
23
23
:34
:56
:06
:10
;20
;39
:43
:47
:54
:09
:13
RO
RO
RO
RO
RO
RO
RO
RO
RO
32-
1,
1.
2.
2,
2,
1,
1.
0,
1,
0.
0.
2.
3,
1,
2.
1.
3.
0,
— ADOV
-1.78
.89
.48
.41
.72
.22
.78
.59
.57
.76
.63
.58
.10
.16
.54
.77
.19
.06
.34
Peaks
0
22
22
22
:00
:18
:28
;52
1,
RO
RO
e: retiir / fes_ULi roj.j.ows •
0.885-1.034
2
72
0
2
2
47
26
1
20
1
1
5
0
0
1
2
0
0
167
.01
.38 43.17
.99
.09
.50
.61 30.48
.99 16.58
.10
.37 12.98
.48
.15
.53
.48
.89
.22
.55
.79
.46
.35
,32-1.78
11
1
1
0
.40
.49
.68
.93
Peaks
aHrnj
0
3,607
327
3
3,938
•a • *D*af""T"l
.13
.44 2,158.35
.56 205.48
.61 2.20
.61
,n / wv-nriT? sr/^1 1 <-^e —
0
29.21 0
0
0
0
17.13 0
10.41 0
0
7.39 0
0
0
1
1
1
1
1
1
1
.000
.893
.914
.921
.926
.939
.957
.967
.984
.991
.994
.001 12378-PeCDD
.016
.019
.022
.027
.038
.041
0.821-1.179
0
1,449.09 1
122.08 1
2.36 1
.000
.000 13C12-PeCDD 123
.007
.025
HXCDF
374-376
M
M
M
374-376
13C12-HXCDF
384-386
AN
1.05-1.43
DC NL 0:00 RO 0.86
01
05
67
60
DC SN
24:07 RO
24:16
24:37 RO
25:14 RO
25:22
25:55
5 Peaks
15
27
0,43-0.59
DC NL
DC SN
0:00 RO
24:05
24:16 RO
25:13
25:20
25:28 RO
25:37 RO
25:55
26:41
0.90
0.58
0.60
0.48
0.48
0.62
1.00
0.49
0.47
2.15
9.18
18.58
0.94
12.92
8.25
7.33
56.26
1.76
15.88
14.49
2,523.84
4,624.35
25.12
1.81
2,704.68
2,266.08
2,158
205
.35
.48
2.20
1,449
122
2
' Follows
5
9
9
4
4
5
5
823
1,492
10
886
728
.08
.53
.26
.41
.10
.80
.74
.59
.67
.30
.90
.36
5
9
5
3
3
10
9
1,700
3,131
16
1,817
1,537
.09
.08
.36
1
1
1
.000
.007
.025
13C12-PeCDD :
0.945-1.064
0.000
.03
.05
.77
.84
.23
0.
.08
.61
.25
.68
.65
.78
.72
0
0
0
0
1
1
.952
.958
.972
.996
.001
.023
123478-HxCDF
123678-HxCDF
23467 8-HxCDF
842-1.158
0
0
0
0
1
1
1
1
1
.000
.951
.958
.995
.000
.005
.011
.023
.053
13C12-HXCDF .
13C12-HXCDF
13C12-HXCDF
13C12-HXCDF
IS3
AN
AN
AN
Triangle Laboratories, Inc.® Analytical Services Division
801 Caprtola Drive • Durham, North Carolina 27713
Phone: (919) 544-5729 • Fax: (919) 544-5491
Printed: 15:5211/11/96
140
-------
Page No.
11/11/96
Listing of T966603B.dbf
Matched GC Peaks / Ratio / Ret. Time
Compound/
M_Z.... QC.Log omit Why ..RT. OK Ratio Total.Area... Area.Peak.1.. Area.Peak.2. . Rel.RT Compound.Name. . ID..
384-386
HxCDD
390-392
390-392
13C12 -HxCDD
402-404
402-404
HpCDF
408-410
M
D
408-410
13C12 -HpCDF
418-420
418-420
26:52
8 Peaks
DC NL 0:00
24:45
25:16
25:31
DC SN 25:37
DC SN 25:56
DC SN 26:06
DC SN 26:12
DC SN 26:29
DC WH 26:40
3 Peaks
DC NL 0:00
25:30
26:05
26:10
26:29
4 Peaks
DC NL 0:00
28:20
D SN 28:41
DC SN 29:02
DC SN 29:07
1 Peak
DC NL 0 : 00
28:18
29:34
2 Peaks
RO 0.83
1
1.05-1.43
RO 0.75
1.29
1.35
1.34
RO 0 . 52
RO 4.13
1.07
RO 0.69
RO 1.61
1.17
1.05-1.43
1.15
1.09
1.25
1.23
1.24
0.88-1.20
1.05
0.91
RO 2.67
RO 0.83
RO 0 . 62
0.37-0.51
RO 0.89
0.42
0.43
5.56 3.06
2,180.00
2.34
7.01 3.95
59.73 34.26
11.28 6.46
0.65
1.05
1.47
1.28
2.31
2.15
78.02
3.23
8.57 4.46
1,953.00 1,084.26
4,031.32 ' 2,219.91
2,354.11 1,303.31
8,347.00
! flxC.!)!) / HpCD? rOXJlOWS ~~
1.91
16.62 7.93
2.90
0.57
0.57
16.62
3.06
3,446.00 1,020.41
1,588.69 481.13
5,034.69
• WTVT1P / HrV^nrj Vr\l 1 nw
-------
Page No.
11/11/96
Listing of T966603B.dbf
Matched GC Peaks / Ratio / Ret. Time
Compound/
H_Z QC.Log Omit Why ..RT. OK Ratio Total.Area— Area.Peak.1.. Area.Peak.2.. Rel.RT Compound.Name.. ID..
424-426
2 Peaks
26.52
13C12-HpCDD 0.88-1.20
436-438 DC NL 0:00 RO 1.22 3.12
28:36 1.16 12.20
29:14 1.05 3,228.98
436-438 2 Peaks 3,241.18
6.54
1,656.41
0.966-1.034
0.000
5.66 0.978
1,572.57 1.000 13C12-HpCDD 678 IS7
OCDF
442-444
442-444
DC
NL 0:00
31:47
1 Peak
/uji
0.76-1.02
0.94
0.81
Above: HpCDD / Octa-CDD and CDF Follows
2.91
10.63
10.63
4.75
0.874-1.126
0.000
5.88 1.003 OCDF
OCDD
458-460
458-460
0.76-1.02
DC NL 0:00 RO 0.64
31:43 0.76
1 Peak
1.13
38.50
38.50
16.64
0.874-1.126
0.000
21.86 1.001 OCDD
AN
13C12-OCDD 0.76-1.02
470-472 DC NL 0:00 RO 0.07 0.06
31:42 0.84 4,577.17
470-472 1 Peak 4,577.17
2,092.57
0.995-1.006
0.000
2,484.60 1.000 13C12-OCDD
IS8
Column Description "Why" Code Description QC Log Desc.
M_Z -Nominal Ion Mass(es)
..RT. -Retention Time !mm:ss)
Rat.l -Ratio of M/M+2 Ions
OK -RO=Ratio Outside Limits
Rel.RT-Relative Retention Time
*** End of Report ***
WL-Below Retention Time Window
WH-Above Retention Time Window
SN-Below Signal to Noise Level
-------
CO
File:T966603 il-835 Acq:31-OCT-1996 23:42:52 EI+ Voltage SIR 70T
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Sample Text:23A-3 TLI#39291R1 INJ. TIME = 23:46 File Text:23A-3 TLIt39»
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File:T966603 #1-835 Acq:31-OCT-1996 23:42:52 EI+ Voltage SIR 70T
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Sample Text:23A-3 TLIf3929lRl INJ. TIME = 23:46 File Text:23A-3 TLI#39»
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331.9368 F:2 Exp:EPCUS
Sample Text:23A-3 TLI#3929lRl INJ. TIME = 23:46 File Text:23A-3 TLI#39»
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-------
File:T9666S3 #1-835 Acg:31-OCT-1996 23:42:52 EI+ Voltage SIS 70T XO±»esl868
303.S016 Ft2 BSUB(256,30,-3.0) PKD(5,3,1,0.10%, 7472.0,0.00%,F,T) ExpiEPCUS
TRIANGLE LABS Tsxt:23A-3 TU#39291X1 IJKT. TIME - 23:46
1003, A1.03E6
80:
60:.
40:
20:
01
A2.14E5
Bl.54E5
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r±leiT966603 #1-835 Acg:31-OCT-1996 23:42:52 EI+ Voltage SIR 70T Hoise-,1947
305.8987 T:2 BSUB(256,30,-3.0) PKD(5,3,1, 0.10%, 7788.0,0. OQ\,F,F) Exp:EPCUS
TRIANGLE LABS Texts23A-3 TLIt39291Rl ISJ. TIME = 23:46
1004 Al,f6E6
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40.
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A2.73S5
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13:00 14:00 15:00 IS:00 17:00
File:T966603 #1-835 Acg:31-OCT-1996 23:42:52 EI+ Voltage SIS 70T Noiae:875
315.9419 T:2 BSUB(25S,30,-3.0) PKD{5,3,1, 0.101,3500, 0,0.00%, F,F) Exp:EPCUS
TRIANGLE LABS Text:23A-3 TLI#3929lRl IJKT. TIME = 23:46
100* A3.05B7
80:
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13:00 14:00 15:00 16:00 17:00
FileiT966603 #1-835 Acq:31-OCT-1996 23:42:52 EI+ Voltage SIS 70T No±se:1232
317.9389 F:2 BSUB(256, 30, -3.0) PKD(5, 3, 1, 0.10%,4928. 0,0.00%, F,F) ExpsEPCUS
TRIANGLE LABS Texts 23 A-3 TLX#39291S1 OKT. TIME = 23s 46
100* A4.J.4S7
so:
401
201
13:00 14:00 15:00 16:00 17-00
FilsiT96S603 #1-835 Acqs31-OCT-1996 23:42:52 EI+ Voltage SIS 70T
330.9792 F:2 Exp:EPCtJS
TSIANGLE LABS Text.-23,8-3 TLI#39291R1 JWT. TIME = 23:46
15:52 16:28 16:51
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13:00 14:00 15:00 16:00 17:00
J-ile:r566603 #1-835 Acqs31-OCT-199S 23:42:52 EI+ Voltage SIS JOT
375,8364 f:2 ExpiEPCtTS
TRIANGLE LABS T&rt:23A-3 TLH39291R1 IIKJ. TIME - 23:46
100*
14:00
LO.OEO
18:00 Time
2.6E5
-.2.1E5
":1. 6E5
.1. OE5
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18:00 Tiae
7. 2E6
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18:00 Time
-3.3E7
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ll.3E7
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18\00 Time
13:00
14 i 00
15:00
16:00
17:00
.O.OEO
18:00 Time
144
-------
ile:T966603 #1-835 Acq:31-OCT-199S 23:42:52 EI+ Voltage SIR JOT H6iae:667
19.8965 T:2 BSm(2S6,30, -3.0) PXS(5, 3,1, 0.10%,-M68.0,0.00%,J', F) ElpsEPCUS
TRIANGLE LASS TfUt:23A-3 TLH39291R1 TOT. TIME - 23:46
004 Al. 04E6
14:00 15:00 16:00 17:00
F±lesT966603 #1-835 Acq[$31-OCT-1996 23:42:52 EI+ Voltage SIS 70T Soiae:828
321.8936 T:2 BSUB(256,30,-3.0) PKD(5,3,1, 0.10^,3312.0, 0. 00\,F,F) SxpsEPCOS
TRIANGLE LASS Text:23A-3 TLH39291R1 INJ. TIME = 23:46
100SA1.3SE6
sol
14:00 15:00 16:00 17:00
FilenT966603 #1-835 Acq:31-OCT-1996 23:42:52 EI+ Voltage SIR 70T No±se:2744
331.9368 F:2 SSUB(256,30,-3.0) PKS(5, 3,1, 0.10%,10976, 0, Q. 00\,F,T) SxpsEfCUS
TRIANGLE LABS Teit:23A-3 TLI#39291R1 Itrj. TIME " 23:46
1004 A2.75E7
40
201
A5.14E5
A2.94ES
A3.62E4
S « ^^J&
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SO-
40:
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A3.58E5
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60
401
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14:00 15:00 16:00 17:00
F±le!T966603 #1-835 Acq;31-OCT-1996 23:42:52 SI+ Voltage SIR 70T Sbise.-$40
333,9338 F:2 BSOB(256,30, -3.0) PKD(5r3,l, 0.10%, 3760. 0,0. 00%, r,T) Exp-.EPCOS
TRIANGLE LABS Texts23A-3 TLI#39291S1 IJKT. TIME « 23:46
1001 A3.51E7
SQL
601
401
201
01
A2.01E7
14:00 15:00 16iOO 17:00
F±le:T966603 #1-835 Acg:31-OCT-1996 23:42:52 EI+ Voltage SIR 70T &alae:525
327,8847 F:2 BSUB( 256, 30, -3. 0) PKD( 5,3,1, 0.10\,2100. 0, 0. 00%, r,F) Exp-.EPCUS
TRIANGLE LABS Teit:23A-3 TLI#39291S1 INJ. TIME ** 23:46
1001 A3.J.2E7
601
401
201
O
14 ,"00 15.-00 16-00 17-00
File:T966603 #1-835 Acq:31-OCT-1996 23:42:52 EH- Voltage SIR 70T
330.9792 F:2 Exp:EPCUS
TRIANGLE LABS Teiti23A-3 TLX#39291R1 TKT. TIME " 23:46
14^23 .±lA°*J&l?AS:37 15:52 J6^« _4£-5117;08 ,7.jg
1001
801
601
401
201
01
14:00
15:00
16:00
17:00
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18:0
7
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Time
-6.2E6
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1.2.5E6
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' Time
'•-6.3E6
'•.4.7E6
13.2E6
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-------
File:T966603 #1-835 Acq:31-OCT-1996 23:42:52 EH- Voltage SIR 70T Noise: 494
339.8597 F:2 BStJB(256, 30, -3.0) PKD(5,3, 1,0. 101,1976.0,
TKIASGLE LABS Text:23A-3 XLHt39291Sl
1003
aol
601
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201
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IKT. TIKE - 23:45
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-.4.8E4
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'21:0o' '22:00 ' ' '23:00' ' ' Time
File:T966603 #1-835 Acq:31-OCT-1996 23:42:52 EH- Voltage SIS 70T Koiaes9S9
341.8567 F:2 BSUB( 256,30, -3 .0 ) PKD(5, 3,1, 0.10%, 3836. 0,
TSIAS5LE LASS Text:23A-3 TLI#39291S1
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401
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File:T966603 #1-835 Acq:31-OCT-1996 23:42:52 EI+ Voltage SIR 70T Itoise:203
351.5000 F:2 BSVB(256r30,-3.0) PXD(5, 3, 1,0. 101,812. 0,1
TRIANGLE LABS Text:23A-3 TLI#39291R1
100S
aol
6ol
40:
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JMJ. TIKE * 23:46
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'21 too' ' 22:00 23:00' ' ' Time
FileiT966603 #1-835 Acq:31-OCT-1996 23:42:52 EH- Voltage SIR 70T Sbise:429
353.8970 F:2 BSUBf 256, 30, -3 . 0) PKD(5,3,1, 0.10%, 1716. 0
TRIANGLE LABS Tezt:23A-3 TLH39291R1
100$
aol
'.
60^
401
201
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JKT. TIKE - 23:46
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file:T966603 #1-835 Aoq:31-OCT-1996 23:42:52 EH- Voltage SIR 70T
330.9792 F:2 Sip:EPCUS
TRIANGLE LABS Text:23A-3 TLI#39291R1
1003
80_
60,
40.
20.
0.
^^^la^lBiasJ? 19:05 19:3619,55 20:32
18:00 19:00 20:00
JKT. TIKE = 23:46
C3.2E7
-2.6E7
"-1.9E7
11 . 3E7
•-6.5E6
• 0 . OHO
21:00 22:00 23:00 lime
File:T966603 #1-835 Acq:31-OCT-1996 23:42:52 EH- Voltage SIR 70T
409.7974 F:2 Exp:EPCUS
TRIANGLE LASS Text:23A-3 TLI039291R1
1003
80.
60.
40.
20.
0
19:11
1
18:41 3l
18:17 | J8.5J I jj j
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18:00 15:00 20:00
JKT. TIKE - 23:46
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14
-------
Flle:T9S6'603 #1-835 Acq:31-OCl-l9S6 23:42:52 Et-f Voltage StS 70f Jfeiae; 747
355.8546 T:2 BSUB(256,30,-3.0) PKD(5, 3, 1,0, 101,2988. 0,0.001,?,*) Elp:EPCUS
TRIANGLE LABS Text: 23 A- 3 TLH39291K1 JWT. TIME = 23:46
IOCS
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20:00 21:00 22:00 23:00 Tine
File:T966603 il-835 Acq:31-OCT-1996 23:42:52 EI+ Voltage SIS 70T Koise:396
357.8516 r:2 BSUB(2S6r30,-3.0) PKD(5r3,l,0. 101,1584 , 0,0,00%, F,F) Exp:EPCUS
TSIAXSLE LASS Texts23A-3 TLI039291S1 JKT. TIME = 23:46
looa
ao:
so:
40:
20:
0"
A2.92E5
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-------
File:T966603 #1-505 Acg:31-OCT-1996 23:42:52 EH- Voltage SIR 70T MoiBe:593
373.8208 Ti3 BSVB(256,30, -3. 0} PKD(5,3,1, 0.101,2372, 0, 0 . 00%,r,F) ExpiEPCVS
TRIANGLE LABS Text:23M-3 TLI039291R1 IJKT. TIMS - 23s46
100* A9.53E4
A3.57E4
24:00 25:00 26:00
FileiT966603 #1-505 Acq:31-OCT-1996 23:42:52 EI+ Voltage SIX 70T Noisei688
375.8178 T:3 BSVB(256, 30, -3. 0) PKD(5,3,1, 0,101,2752.0,0. 00%,T,F) Exp-.EPCUS
TRIANGLE LABS Text:23A-3 XLH39291S1 IJST. TIKE - 23:46
IOCS A9.Q5E4
24-00 25:00 26:00
File:T966603 #1-505 Acq:31-OCT-1996 23:42:52 EH- Voltage SIR 70T Noise:52S
383.8639 F:3 BSV3(25S, 30, -3.0) FXDfS, 3,1,0.10%,2104, 0,0.00%,F, f) ExpsEfCUS
TRIANGLE LASS Text:23A-3 TLH39291R1 IWJ. TIME = 23:46
10 OS, A1.49E7
A4.83E3
27:00
27:00
80:
6ol
401
20:
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A8.87E6
A7.28E6
24:00 25:00 26:00
File:T966603 #1-505 Acq:31-OCT-1996 23:42:52 EH- Voltage SIR 701 No±se:586
395.8610 F:3 BSVB(256,30, -3.0) PKD(5,3fl,0.10%,2344.0,0.00^,F,F) Exp:EPCUS
TRIANGLE LABS Text:23A-3 TLI#39291R1 IJKT. TIME = 23:46
1004 A3.13E7
27:00
8 01
601
401
201
Al.82E7
Al.54E7
24:00 25:00 26:00
F±le:T966603 #1-505 Acq:31-OCT-1996 23:42:52 EH- Voltage SIX 70T
392.9760 F:3 Exp:EPCUS
TRIANGLE LASS Text:23A-3 TLI#3929lRl UKT. TIME »
24:10 24••27^4J(40 .^t^vi. 25:1325:25 _25:5S26:10
80J
601
401
201
01
27:00
23:46
26:28
24:00 25:00 26:00
File:T9666Q3 #1-505 Acq:31-OCT-1996 23:42:52 EH- Voltage SIX 70T
445.7555 F:3 ExptEPCVS
TRIANGLE LABS Text:23A-3 TLI#39291R1 IMi7. TIME =
1001
27:00
23:46
.3.5E4
.2.8E4
.2.1S4
.1.4X4
.7.0E3
.O.OEO
Tiffle
.3. 6E4
2.9E4
2.2E4
1.5E4
7.3E3
.O.OEO
Time
.4.3E6
.3.5E6
.2.6E6
.1. 7E6
.8.7E5
.O.OEO
Time
.9.3E6
.7.4E6
.5.6E6
.3.7E6
.1. 9S6
.O.OEO
Time
.1. 6E7
.1.3E7
.9.7E6
.6.5E6
.3.2E6
.O.OEO
Time
24:00
251 00
26} 00
27:00
J43
-------
'ile:T966603 #1-505 Acqi31-OCT=195S23:42:52 EI+ Voltage sts 701 lkiae:644
BS.8156 FsJ BStJ3(256,30r -3.0) PXB(5,3,1,0,10*,2576. 0,0.00%, f,f) SxpsEPCUS
TRIANGLE LABS Texti23A-3 TLH39291S1 INJT. TIKE - 23:46
IOCS A3.43ES
801
601
24':36 24:48 25:00 25:12 25:24 25:36 25:48 26:00 26:12 26:24 26:36 26:48
Pile:T966603 #1-505 Acq:31-OCT-1996 23:42152 EH- Voltage SIS 70S Mais*:866
391.8127 F:3 BSUB(256,30,-3.0) PKD(5r 3,1,0.101,3464. 0,0.00%, ?,?) Elp:EPCUS
TBIANSLS LASS Teit:23A-3 TZI#39291M1 IKT. TIME " 23:46
1004 A2.55ES
aoi
24:36 24:48 25:00 25:12 25:24 25:36 25:48 26:00 26:12 26:24
File:T966603 #1-505 Acq:31-OCT-1996 23:42:52 EH- Voltage SIS 70T Noise:865
401.8558 F:3 BStTB(256,30, -3. 0) PKD(5,3,lr 0.10%,3460.0, 0.00*,FrF) Exp:EPCUS
TRIANGLE LASS Text:23A-3 TLI#39291M1 XM7. TIME = 23:46
1004 A2.22E7
401
201
A3.9SX4
ii^u- AY v^_-«—I-**..
Al.66E4
A.
20.
A4.82E4
fS\A6.92E3 A4-^3 A7.14E3 A1.47E4
A9.88E3
26:36 26:48
801
601
401
201
A1.30E7
24:36 24:48 25:00 25:12 25:24 25:36 25:48 26:00 26:12 26:24 26:36 26:48
File:T966603 #1-505 Acq:31-OCT-1996 23:42:52 EH- Voltage SIX 70T Noise: 751
403.8529 F:3 BSUB(256, 30, -3. 0) PKD(5, 3,1, 0 .10%, 3004 . 0, 0. 001,F,F) Exp:EPCUS
TRIANGLE LASS Text:23A-3 TLI039291S1 UU. TIME = 23:46
IOCS A1.S1E7
801
601
401
201
Al. 05E7
24:36 24:48 25:00 25:12 25:24 25:36 25:48 26:00 26:12 26-24 26:36 26:48
file;T966603 #1-505 Acq:31-OCT-lS96 23:42:53 EH- Voltage SIX 70T
392.9760 F:3 EXpiSPCUS
TRIANGLE LASS Text:23A~3 TLI#39291M1 UKT. TIME - 23:46
so:
so:
401
201
a.
26:28
26:38 26:48
.1.1E5
,8,714
.S.5E4
.4.3E4
.2. 2E4
.O.OEO
Time
.8.8E4
.7.0E4
.5. 3E4
. 3.5E4
.1. 8E4
' | •"j"»T«'r—* inf«r , ,=
-------
File 13-966603 #1-443 Ac?s31-OCT-1996 23.-42.-52 EI+ Voltage SIS 701 Noise:488
407.7818 F:4 BSUB(256r30, -3. 0) PKB(5,3,1, 0.101,1952.0,0, 00%,F,F) ExpsEPCOS
TSIANGLE LASS Te4tt.-23.S-3 TLI«39291X1 JKT. TIME = 23:46
1001
so:
60:
28:12 28:24 28.-36 28:48 29:00 29.-12 29:24 29:36
File:T966603 41-443 Aoq:31-OCT-1996 23:42:52 EH- Voltage SIX 70T Soiae:467
409.7789 F:4 BSOS(256,30, -3.0) PKD(5,3,1,0.101,1868.0,0.00*,F,F) Exp:EPCUS
TRIANGLE LABS Texti23A-3 TZI#39291X1 JKJ. TIME = 23:46
100*
28-12 28:24 28:36 28:48 29:00 29:12 29:24 29:36
File:T966603 #1-443 Acq:31-OCT-1996 23:42:52 EH- Voltage SIX 70T Noise:944
417.8253 F:4 BSVS(256,30, -3. 0) PJOJf 5, 3,1, 0.10%, 3776. 0, 0, 00\,T,T) Exp:EPCUS
TRIANGLE LABS Text:23A-3 TLI#39291X1 X«J. TIME = 23:46
lOOt A1.Q2S7
40:
20:
A6.02E4
/w
A3.79E4
A
P
7.17E3
29:48
29s48
ao:
60:
40:
20:
oj
A4 . 81E6
28:12 28:24 28:36 28:48 29:00 29:12 29:24 29:36
F±le:T966603 #1-443 Acg.-31-OCT-1996 23:42:52 EI+ Voltage SIR 70T Noise:1062
419.8220 F:4 BSUB(256,30,-3 .0} PKS(5,3,1, 0.10%, 4248. 0,0. 00*,F,F) Exp:EPCOS
TRIANGLE LABS Texts23A-3 TLIif39291Rl JKT. TIME - 23:46
1004 A2.43E7
80:
60:
40.
20:
29 -48
o:
A1.1J.S7
28:12 2fls24 28:36 28:48 29.-00 29:12 29:24
File:T966603 #1-443 Aeg-;31-OC3'-1996 23:42:52 EH- Voltage SIX 70T
430.9729 Fs4 Exp:EPCUS
TRIANGLE LABS Texts23A-3 TLI#39291R1 XH7. TIME
1003, 28:15 28:25
29:36 29:48
23:46
28-12 28:24 28:36 28:48 29:00 29:12 29:24
File:T966603 #1-443 Acq:31-OCT-1996 23:42:52 EH- Voltage SIS 70T
473,7165 F:4 SxpiEPCUS
TRIANGLE LABS Textt23A-3 TLI#39291R1 XKT. TIME
23s46
28il2
28:24
28:36
28.-48
29QO
29:12
29:24
-8.2E4
16.3E4
L.4. 1JE4
12.1JET4
JO.- 00
LO.OSO
Tiae
-4.6E4
JO: 00
,-2.7E6
_2.0£6
.1,4E6
|- o - ngn
30:00 Time
ra.iE6
L6.5E6
13.2E6
.1. 6E6
.O.QEO
30:00 Time
-1.1E7
'
3ooo
-------
-------
File:T966603 #1-443 AcqT31-OCT-1996 23:42:52 EI+ Voltage SIR 70T
441.7428 F:4 BSUS(256, 30,-3.0) PKDf 7,2,3, 0.10^,2824. 0, 0. 00%,t,t)
TSIMtSLS LABS Texts23A-3 TLI#39291S1 IKT.
1001
29:00 30:00 31:00
F±ie:T966603 #1-443 Acq:31-OCT-1996 23:42:52 EX+ Voltagre SIS 7QT
443.7399 F:4 BSUB(256,30, -3. 0) PKB(7,2,3,0.10\,2996, 0,0.00%,F,F)
TRIANGLE LABS Text:23A~3 TLI#39291S1 IKT.
100* AS
Wbise:706
ExpiEPCUS
TIMS = 23:46
32:00
Soiae:749
ExpsEPCUS
TIME = 23:46
8E4
33:00
29:00 30:00 31:00
F±le:T966603 #1-443 Acqi31-OCT-1996 23:42:52 EI+ Voltage SIR 701
430.9729 F:4 ExpsEPCUS
TMIAJfGLE LABS Texts23A-3 TLI#39291X1 IJKT.
30i22 i 30:4731:06
SOJ
sol
701
sol
501
401
301
201
101
01
32:00
TIME ~ 23:46
"?;?JL 32:27
33:00
29:00 30:00 31:00
File:T966603 #1-443 Acqs31-OCT-19S6 23:42:52 EI+ Voltage SIS 70T
513.6775 F:4 ExpiEPCUS
TRIANGLE LASS
1004
Teit:23A-3 TLI#39291S1
32:00
IJKT. TIME = 23:46
33:00
1.1E7
9.7E6
8.6E6
7.6E6
6.5E6
5. 4E6
4.3E6
3.2E6
.2.2E6
.1, 1E6
o. OEO
Time
29:00
30:00
31-00
32:00
33:00
152
-------
iletf9S6603 #1-443 Acq:31-ocf-15ffS 23:42:52 SI+ Voltage Sts 70? W>iae:2S5
57.7377 f:4 BSUB(256, 30, -3. 0) PXD( 7,2,3, 0.101,1060.0,0, 00\,F,F) ExpsEPCUS
TRIANGLE LABS Texts23A-3 TLI#39291X1 JJKT. TIMS - 23:46
COS Al. 66E5
801
32:06
31:36 31:42 31-.4S 31:54 32:00
F±lesT966603 #1-443 Acqs31-OCT-1996 23:42:52 EI+ Voltage SIS 70T No±ae:415
459.7348 f:4 SSUS(256,30,-3.0) PKB( 7,2, 3, 0.10*,1660. 0, 0. 00%,f ,F) SxpiEPCUS
TRIANGLE LABS Text:23A-3 TLI#39291K1 IJfiT. TIME - 23:46
1004 A2.J.SE5
-S.SE4
'.5.5E4
".4.2E4
".2.8E4
-1.4E4
.O.OEO
32:12 Time
_S,5JE4
32:05
31s 36 31:42 31:48 31-54 32'tOO
FileiT966603 #1-443 Acq:31-OCT-1996 23:42:52 EI+ Voltage SIB JOT Noise:17
469.7779 F:4 SSUS( 256,30, -3 . Oj PXE(7,2,3, 0.101,68.0, O.Q01,F,F) Exp-.EPCUS
TSIASSLE LABS Text'.23A-3 TLI039291K1 JK7. TIME - 23:46
IOCS, A2.
8C
so:
40:
201
-O.OEO
32J12 Time
7.2E6
".5.BE6
-4.3E6
'.2.9E6
11.4E6
.O.OEO
32: OS
31:36 31:42 31:48 31:54 32:00
File:T966603 §1-443 Acq:31-OCT-19S6 23:42:52 EI+ Voltage SIS 70T !To±ses226
471.7750 F:4 BSUB(256,30,-3.0) PKD(7,2,3,0.10^,904.0,0. QO\,FrF) Eip:EPCUS
TRIANGLE LABS Texts23A-3 TLI#39291S1 ' XWJ. TIME = 23:46
IOCS A2.4JIE7
32:12 Time
B,5E6
'.6.8E6
.5.1E6
".3. 4E6
'.1.7E6
31:36 31:42 31:48 3Ji54 32'sOO 32:06
File:T966603 #1-443 Acqs31-OCT-1996 23:42:52 EI+ Voltage SIK 70T
430.972S F:4 Exp:EPCUS
TXIANSLS LABS Text:23A-3 TLI#392S1R1 XWJ. TIME - 23:46
100* -3-Lii! 31:52 31.-56 32jJ)4 32:08
80.
60.
401
20.
0.
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32:12 Time
rl.lE7
"-8.4E6
'.S.3E6
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".2.1E6
31:36
31s 42
31:54
32tOO
, — , i
32s 06
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Time
3
-------
tef, iass 282.3^ Peak top
Htlgt §,81 volts Span 896 spa
Systei file naie
Data file naie
Resolution
Grajptuarer
lonizatlon
Switchutg
ief,
y
I y
m
384
m
318
318
329
m
m
33!
331
332
334
348
342
382
354
38
EPCUS
y 3?s
v 4ia
Chamsi I 31,3/iE Peak top
4.4S yolts Span 288 i
-------
I.-5
File:T966603 #1-835 Acq:31-OCT-1996 23:42:52 El-f Voltage SIR 70T
303.9016 F:2 Exp:EPCUS
Sample Text:23A-3 TLI#39291R1
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14:12 14:18 14:24 14:30 14:36 14:42 14:48 14:54 15:00 15:06 15:12 15:18 15:24 15:30
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L5.3E4
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Time
File:T966603 #1-835 Acq:31-OCT-1996 23:42:52 EH- Voltage SIR 70T
305.8987 F:2 Exp:EPCUS
Sample Text:23A-3 TLI#39291R1 INJ. TIME = 23:46 File Text:23A-3
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315.9419 F:2 Exp:EPCUS
Sample Text:23A-3 TLI#39291R1 INJ. TIME = 23:46 File Text:23A-3
100%
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15.4E4
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Time
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14:38
15:11
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14:12 14:18 14:24 14:30 14:36 14:42 14:48 14:54 15:00 15:06 15:12 15:18 15:24 15:30 Time
File:T966603 #1-835 Acq:31-OCT-1996 23:42:52 EI+ Voltage SIR 70T
317.9389 F:2 Exp:EPCUS
Sample Text:23A-3 TLIf3929lRl INJ. TIME = 23:46 File Text:23A-3 TLIf39»
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File:T966603 #1-835 Acq:31-OCT-1996 23:42:52 EI+ Voltage SIR 70T
305.8987 F:2 Exp:EPCUS
Sample Text:23A-3 TLI#39291R1 INJ. TIME = 23:46 File Text:23A-3 TLI#39»
100% _ _1.6E5
50:
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315.9419 F:2 Exp:EPCUS
Sample Text:23A-3 TLI#3929lRl INJ. TIME = 23:46 File Text:23A-3 TLI#39»
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File:T966603 #1-835 Acq:31-OCT-1996 23:42:52 EI+ Voltage SIR 70T
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File:T966603 #1-835 Acq: 31-OCT-1996 23:42:52 EI+ Voltage SIR 70T
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Sample Tex_ti23A-3 TLIt3929lRl INJ. TIME = 23:46 File Text:23A-3 TLI#39»
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Sample Texti23A-3 TLIt3929lRl INJ. TIME = 23:46 File Text:23A-3 TLI#39»
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Time
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File:T966603 #1-835 Acq: 31-OCT-1996 23:42:52 EI+ Voltage SIR 70T
315.9419 F:2 Exp:EPCUS
Sample Text:23A-3 TLI#39291R1 INJ. TIME = 23:46 File Text:23A-3 TLI#39»
100%, 16;04 _8.1E4
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0
16:23 16:40
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Time
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File:T966603 #1-835 Acq:31-OCT-1996 23:42:52 EI+ Voltage SIR 70T
317.9389 F:2 Exp:EPCUS
Sample Text:23A-3 TLI#39291R1 INJ. TIME = 23:46 File Text:23A-3 TLIf39»
100%, 16:03
50jl \ 15.1E4
^\ . J \ 16:41 16:58 n.in 17:35 n.c-3 10.10 1 fl . d7 IQ.A-J t
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18:00
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319,8965 F:2 Exp:EPCUS
Sample Text:23A-3 TLI#39291R1
100% 16;17
15:26
15:48 16:07
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-2.8E4
16:34
17:05
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File:T966603 #1-835 Acq:31-OCT-1996 23:42:52 EI+ Voltage SIR 70T
321.8936 F:2 Exp:EPCUS
Sample Text:23A-3 TLI#39291R1 INJ. TIME = 23:46 File Text:23A-3 TLI#39»
100% 16:17 _4.3E4
501
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15:51
16:35
16:48
17:13
17:35 17:53
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18:00
Time
16:00 17:00
File:T966603 #1-835 Acq:31-OCT-1996 23:42:52 EI+ Voltage SIR 70T
331.9368 F:2 Exp:EPCUS
Sample Text:23A-3 TLI#39291R1 INJ. TIME = 23:46 File Text:23A-3 TLI#39»
100% 16;23 _6.2E6
OJ
16:09
13 . 1E6
.O.OEO
18:00
Time
16:00 17:00
File:T966603 #1-835 Acq:31-OCT-1996 23:42:52 EI+ Voltage SIR 70T
333.9338 F:2 Exp:EPCUS
Sample Text:23A-3 TLI#39291R1 INJ. TIME = 23:46 File Text:23A-3 TLI#39»
100% 16^23 _7.9E6
501
0
16:09
16:00
13.9E6
0. OEO
17:00
18:00
Time
-------
File:T966603 #1-835 Aeq:31~OCT-1996 23752:52 EI+ Voltage SIR TOT Noise;867
319.8965 F:2 BSUB(256,30,-3 . 0} PKD(7,3,1,0.10%,3468.0,0.00%,F,T) Exp:EPCUS
Sample Text:23A-3 TLI#39291R1 INJ. TIME = 23:46 File Text:23A-3 TLI#39»
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File:T966603 #1-835 Acq:31-OCT-1996 23:42:52 EI+ Voltage SIR 70T Noise:828
321.8936 F:2 BSUB(256,30,-3 . 0) PKD(7,3,1,0.10%,3312.0,0.00%,F,T) Exp:EPCUS
Sample Text:23A-3 TLI#39291R1 INJ. TIME = 23:46 File Text:23A-3 TLI#39»
A1.92E5 _4.3E4
A3.50E4
A2.24E4
A1.72E4
12.2E4
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18:00
Time
16:00 17:00
File:T966603 #1-835 Acq:31-OCT-1996 23:42:52 EI+ Voltage SIR 70T
331.9368 F:2 Exp:EPCUS
Sample Text:23A-3 TLI#39291R1 INJ. TIME = 23:46 File Text:23A-3 TLIt39»
100% 16;23 _6.2E6
\J \SJJ
50 1
o:
16:09 /\
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18:00
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16:00 17:00
File:T966603 #1-835 Acq:31-OCT-1996 23:42:52 EI+ Voltage SIR 70T
333.9338 F:2 Exp:EPCUS
Sample Text:23A-3 TLI#39291R1 INJ. TIME = 23:46 File Text:23A-3 TLI#39»
100% 16;23 _7.9E6
16:09
16:00
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18:00
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Time
-------
File:T966603 #1-835 Acq:31-OCT-1996 23:42:52 EI+ Voltage SIR 70T
319.8965 F:2 Exp:EPCUS
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-------
TLI Project: 39291rl
Client Sample: 23A-3
Method 23 TCDD/TCDF Analysis (DB-225)
Analysis File: X964235
Client Project:
Sample Matrix:
TLI ID:
Sample Size:
Dry Weight:
GC Column:
Eastern Ridge Lime Facility
M23TRAIN Date Received:
143-23-3A-C Date Extracted:
Date Analyzed:
1.000
n/a
DB-225
Dilution Factor:
Blank File:
Analyst:
10/19/96
10/21/96
11/01/96
n/a
T966616
JF
Spike File:
ICal:
ConCal:
% Moisture:
% Lipid:
% Solids:
SPC2NF08
XF21266
X964226
n/a
n/a
n/a
2,3,7,8-TCDF
0.03
0.75
20:21
13C12-2,3,7,8-TCDF
6.9
86.0
40%-130%
0.79
20:20
13C12-1»2,3,4-TCDD
0.80
19:23
Data Reviewer td«K^\).uJfc^
11/11/96
Page 1 of 1
C2«LPSRvU4,LARS608.00
Triangle Laboratories, Inc.®
801 Capitola Drive • Durham, North Carolina 27713
Phone: (919) 544-5729 • Fax: (919) 544-5491
Printed: 16:12 11/11/96
1 r> 3
-------
Data Review By:
Initial ....Date...
// / / '/ .Aft calculated Noise Area:
7.00
The Total Area for each peak with an ion abundance ratio outside
ratio limits has been recalculated according to method retirements.
Page No.
11/01/96
Listing of X964235B.dbf
Matched GC Peaks / Ratio / Eet. Time
Compound/
M_Z.... QC.Log Omit Why ..RT. OK Ratio Total.Area... Area.Peak.1.. Area.Peak.2.. Rel.RT Compound.Name.. ID.
TCDF
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16:09
DC SN 16:33
DC SN 16:38
DC SN 16:41
DC SN 16:49"
DC SN 16:50
17:06
17:13
17:18
17:30
17:45
17:54
17:59
18:10
18:19
18:40
DC SN 18:55
19:05
19:21
19:30
19:44
19:51
20:14
20:21
'20:31
20:42
20:51
21:30
DC SN 21:33
DC SN 22 : 02
DC SN 22:06
DC SN 22:12
304-306 22 Peaks
13C12-TCDF
316-318 DC NL 0:00
DC WL 18:42
DC WL 19:05
DC WL 19:19
19:54
20:20
20:50
0.6S-0.89
RO
RO
RO
RO
RO
RO
RO
RO
RO
RO
RO
RO
0.
0.
2.
1.
0.
1.
1.
0.
0.
0.
0.
0.
0.
0.
0.
0.
0.
0.
0.
0.
0.
0.
0.
0.
0.
0.
99
81
84
49
18
39
05
59
80
76
92
67
56
64
74
78
86
18
58
70
72
74
.82
.71
.75
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0.77
0.84
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RO
RO
RO
0.
RO
RO
RO
RO
1.01
1.11
0
0
1
.44
.80
.79
6.
297.
2.
2.
1.
3.
3.
204.
204.
318.
170.
173.
207.
81.
429.
164.
484.
1.
155.
193.
149.
37,
142.
47
09
76
51
90
26
65
59
68
20
37
36
90
61
97
79
16
76
.95
,65
54
.58
,33
133.42
108.81
128.06
95.17
104.84
48.07
3
8
4
1
4,034
.97
.51
.49
.86
.14
133.
88.
90,
137,
88,
69.
90.
35
183
72
223
67
79
62
16
64
55
46
55
41
47
27
.04
.55
.77
,11
.54
.79
.88
.34
.51
.04
.20
.98
.85
.74
.02
.25
.48
.80
.97
,42
.80
.44
164.
151.
113.
181.
96.
103.
161.
55.
246
92
260
116
113
86
21
78
77
62
72
53
57
27
.65-0.89
7
2
1
0
2
0
0
.38
.21
.66
.83
.48
.79
.66
1
15
48
174
25
25,458
266
.26
.20
.50
.31
.25
.30
.91
35
11,236
106
.39
.40
.08
14
14,221
160
0.788-1.094
05
30
.91
.09
.27
.57
.07
.64
.46
.75
.96
.83
.80
.80
.56
.08
.94
.01
.09
.75
.04
.15
0.
.25
.90
.83
0.
0.
0.
0.
0.
0.
0.
0.
0.
0.
0.
0.
0.
0.
0.
0,
0,
0.
0
0
0,
0,
0.
0
1
1
1
1
1
1
1
1
1
000
794
814
818
820
827
828
841
847
851
861
873
880
.884
.893
.901
.918
.930
.939
.952
.959
.970
.976
.995
.001 2378-TCDF
.009
.018
.025
.057
.060
.084
.087
.092
951-1.049
0
0
0
0
0
1
1
.000
.920
.939
.950
.979
,000 13C12-237
.025
Triangle Laboratories, Inc.® Analytical Services Division
801 Capitola Drive • Durham, North Carolina 27713
Phone: (919) 544-5729 • Fax: (919) 544-5491
Printed: 18:461
-------
Page No.
11/01/96
Listing of X964235B,dbf
Matched GC Peaks / Ratio / Ret. Time
Compound/
M_Z.... QC.Log Omit Why .-RT, OK Ratio Total.Area... Area.Peak.1.. Area.Peak.2.. Rel.RT Compound.Name.. ID.,
316-318
DC WH 22:05
3 Peaks
0.74
335.25
25,750.46
1.086
Above: TCDF / TCDD Follows
13C12-TCDD
332-334
332-334
0.65-0.89
DC NL
0:00 RO
18:07
19:11
19:23
20:02 RO
Peaks
1.28
0.80
0.79
0.80
1.03
1.38
74.83
17,448.84
10,676.01
189.56
28,389.24
33.24
7,706.02
4,739.38
110.39
0.896-1.104
0.000
41.59 0.944
9,742.82 1.000 13C12-2378-TCDD IS1
5,936.63 1,010 13C12-1234-TCDD RSI
107.02 1.044
Column Description "Why" Code Description. QC Log Desc.
M_Z -Nominal Ion Mass{es)
..RT. -Retention Time jimtuss}
Rat.l -Ratio of M/M+2 Ions
OK -RO=Ratio Outside Limits
Rel.RT-Relative Retention Time
End of Report
WL-Below Retention Time Window
WH-Above Retention Time window
SN-Below Signal to Noise Level
-------
-------
S1-7M Acer.- i-NOV-1996 IBTlltat OC JBT+ Volkmge i
303.9016 asm(2S6,30,-3.0) PKD(S,3, 1, 0.10%, 7220.0,0. OQ*,F,P)
Sa&plo Text:23A-3 TLI#39291rl File TextiTRIANGLE LABS
iota AJ..
Jfoisc;1805
y 17:00 13:00 15*00 20:00 , 21:00 22:00
PilesX96423S #1-784 Actjt l-NQV-1996 18:11:28 OC EI+ Voltage SIR AutoSpec Noise: 1831
305.8987 BSUB(2S6,30,-3.Q) PKDf 5,3, 1, 0.10*, 7324. 0» 0.00%
Sanple Taxt:23A-3 TLI#39291rl File Text:TRIANGLE LABS
10041 A2.46E6
801
16-00 17:00 18:00 19'sOO 20:00 21:00 22:00
File:X96423S #1-784 Aagi l-NQV-1996 18:11:28 OC EI+ Voltage SIR AutoSpec Noise:2619
315.9419 BSUB(256,30,-3.0) PKD(5,3, 1, 0.10*, 10476.0, O.OOX,P,F) Exp:l
Saiople Texts23A-3 TLI#39291rl File Text:TRIANGLE LABS
IOCS* A1.12E8
801
so:
4 a:
20:
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Fil9tX964235 #1-784 Acg: l-NOV-1996 18:11:28 QC EI+ Voltage SIR AutoSpec NOise:357
317.9389 BS'Ua(25e,30,-3.01 PKO(Sf3, 1, 0.10%, 1428. 0, 0. 00*,F,P)
Saapl* react 123A-3 TLI#39291rl File Text:TRZANOLE LABS
100% A1.42E8
801
601
401
201
0.
22«00
1S-00 17:00 18:00 19:00 20:00
File:X964235 #1-784 Aeg: 1-&OV-1996 18:11:28 OC £1+ Voltage SIR
375.8364 Sxp:XCOHP_TT
Sample Text:23A-3 TLI#39291rl File Text:TRIANGLE LABS
lOOt
21*00
22} 00
so:
601
401
201
0.
16:53
1:07
19:10
O.OEO
Time
.5. OSS
.4.0ES
3.0ES
2. OSS
l.OES
o.oso
Txme
21 111
53.57
17
16 00
17.- 00
16:00
15*00
20:00
21:00
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.0.0£0
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-------
'ile:X9£4235 #1-7B4' Aag: l-NOV-ISSS iBtlltSB ise:3Sl
333,9338 BSUB(256,30,-3.0) FXD(S,3,lf 0.10X, 1564.0, 0.00*,F,F) ExptXCO®F_T?
Simple Taxt:23A-3 TLI#39291rl File Toxt: TRIANOLE LABS
lOOjf MS 74E7
eo:
60.
40.
20.
ft
.94E7
.6. OSS
.4.8E5
.3.6S5
.2.4ES
.1.225
.0.020
Time
.7.525
.5.325
.4.725
.3.225
.1.625
.0.020
Time
.2.027
Ll.«27
.1.227
.7.9E6
14.0E6
17iOO
18100
19 i 00
20iOO
21:00
.O.OEO
Time
.1.527
.1.227
.S.12S
.6.1E6
.3.0E6
.O.OEO
.1.527
.1.527
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.7. 72$
.3.82S
.O.OEO
Tine
173
-------
FileiX964235 #1-784 Acg; 1-M3V-15S6 18*11*28 OC BI+ Voltage SIR
303.9016 Exp:XCOOF_TT
Sample Texts23A-3 TLI#39291xl File Text s TRXAKOLE LABS
100* • as 40
•
80:
eo:
•
40:
I
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0'
18*10
t
A 1 7: 54 P\ \
A A AH j A 1 1 \ i A i 30i
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16:00 ' ' ' 17*00 ' ' ' 18*00 ' ' 15*00 ' ' ' 20:00
PilesX96423S #1-784 Acq; l-SOV-1996 18*11*28 OC EX* Voltage SIR
315.9419 Exp:XCOSF_TT
Sample 5"«rt;23A-3 ?tX#3S251rl Pile Text * TSIASOLS LAMS
IOCS
so:
60:
40:
20:
o:
20
16*00 17*00 18*00 15*00 20*00
Fil»iX96423S #1-784 Jlcg* 1-W5V-15S6 1S*11."2S SC EX* Voltage SIR
319.8965 Exp:XCONF_TT
Saople T«rt.-23A-3 H,I#352Slrl Pile Text : TRIANGLE LABS
IOCS
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20:
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A
M 18*05
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FilesX964235 #1-784 Acq: l-SOV-1996 18:11:28 OC EX+ Voltage SIR
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Sample Text:23A-3 TLI#39291rl File TextsTRIASOLE LABS
100*
BO!
60-
401
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0:
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1
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16-00 ' ' ' 17*00 ' ' ' 18*00 ' ' ' 15*00 ' ' ' 20*00
File:XS6423S #1-784 Acq: l-SOV-1996 18:11:28 OC EX* Voltage SIS
252.5825 Exp : XCONF_TT
Sasple Text:23A-3 TLI#39291rl File TextsTRZAWiLE LABS
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60.
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0.
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A A i A 21*30
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M J \. >U \ Jl 22*02
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Sample Text:23A-3 TLI#39291rl File Text s TRIANGLE LABS
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80.
60.
40.
20.
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^^ w«s*«V'V~~ >->A«— ^ ^ Jlr W~~^WMrt~^^v^vv
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• o.oso
ili-od ' ' 22sOO ' ' Time
174
-------
Peak Locate Examination: 1-NOV-1996:18:11 File:X964235
Experiment:XCONF_TT Function:1 Reference;PFK
j-.-v.
-I
CJI
-------
TLI Project: 39291rl
Client Sample: 23B-1
Method 23 PCDD/PCDF Analysis (a)
Analysis File: T966604
Client Project:
Sample Matrix:
TLI ID:
Sample Size:
Dry Weight:
GC Column:
Eastern Ridge
M23TRAIN
143-23-4A,8
1.000
n/a
DB-5
Lime Facility
Date Received:
Date Extracted:
Date Analyzed:
Dilution Factor:
Blank File:
Analyst:
10/19/96
10/21/96
11/01/96
n/a
T966616
66
Spike File;
ICal:
ConCal:
% Moisture:
% Lipid:
% Solids:
SPX23708
TF53286
T966598
n/a
n/a
n/a
2,3,7,8-TCDD
1,2,3,7,8-PeCDD
1,2,3,4,7,8-HxCDD
1,2,3,6,7,8-HxCDD
1,2,3,7,8,9-HxCDD
1,2,3,4,6,7,8-HpCDD
1,2,3,4,6,7,8,9-OCDD
2,3,7,8-TCDF
1,2,3,7,8-PeCDF
2,3,4,7,8-PeCDF
1,2,3,4,7,8-HxCDF
1,2,3,6,7,8-HxCDF
2,3,4,6,7,8-HxCDF
1,2,3,7,8,9-HxCDF
1,2,3,4,6,7,8-HpCDF
1,2,3,4,7,8,9-HpCDF
1,2,3,4,6,7,8,9-OCDF
Total TCDD
Total PeCDD
Total HxCDD
Total HpCDD
Total TCDF
Total PeCDF
Total HxCDF
Total HpCDF
Hiiii
::::>:::::¥::::::::x-£:;;:
ND
ND
ND
ND
ND
0.05
0.34
0.16
0.02
0.03
0.04
0.02
0.02
ND
0.07
0.01
0.06
":S$:S*::$:¥?::::*
iiiMp
mrnrnmi
0.20
0.08
0.20
0.09
1.4
0.43
0.16
0.08
0.01
0.02
0.02
0.02
0.02
0.02
5
2 0.17
2
2
12 1.4
10 0.44
5
2 0.10
1.02
0.92
0.78
1.37
1.61
1.27
1.33
1.32
1.13
0.96
0.88
29:14
31:43
15:38 "
20:51
21:51
25:14
25:20
25:56 B_
28:18 ~~~
29:33
31:46
Page 1 of2
X237_PSR vl.U, LARS 6X8.00
Triangle Laboratories, Inc.®
801 Captola Drive * Durham, North Carolina 27713
Phone: (919) 544-5729 • Fax: (919) 544-5491
Printed: 16:0411/11/96
176
-------
TLI Project: 39291rl
Client Sample: 23B-1
Method 23 PCDD/PCDF Analysis (a)
Analysis File: T966604
13e,2-2,3,7,8-TCDF
13C,2-2,3J,8-TCDD
13C12-l)2,3,7,8-PeCDF
13Ci2-l,2,3,7,8-PeCDD
13Ci2-l,2,3,6,7,8-HxCDF
"C,2-l,2,3,6,7,8-HxCDD
13e,2-l,2,3,4,6,7»8-HpCDF
13Ci2-l,2,3,4,6,7,8-HpCDD
!3Ci2-l,2,3,4,6,7,8,9-OCDD
5.8
6.1
5.8
5.3
5.9
6.6
6.5
6.7
11.1
73.0
76.8
72.4
66.1
74.0
83.0
81.6
84.3
69.1
40%-130%
40%-130%
40%-130%
40%430%
40%-130%
40%-130%
25%-130%
25%-130%
25%-130%
0.74
0.79
1.49
1.52
0.48
1.23
0.43
1.04
0.83
15:35
16:22
20:51
22:18
25:20
26:10
28:18
29:14
31:42
37O1-2,3,7,8-TCDD
°C,2-2,3,4,7,8-PeCDF
13ei2-l,2,3,4,7,8-HxCDF
13Ci2-l,2,3,4J,8-HxCDD
i3Ci2-l,2,3,4,7»8,9-HpCDF
4.5
4.4
4.8
4.4
4.4
112
110
121
110
110
70%-140%
70%-140%
70%-140%
70%-140%
70%-140%
1.51
0.48
1.24
0.44
16:23
21:50
25:13
26:05
29:33
13Ci2-l,2,3,7,8,9-HxCDF
13Ci2-2,3,4,6,7,8-HxCDF
4.0
3.8
100
95.9
4Q%-130%
40%-130%
0.48
0.49
26:40
25:55
Recovery Standards
Ratio
ST
Flags
13C,2-1,2,3,4-TCDD
13Ci2-l,2,3,7,8,9-HxCDD
0.81
1.22
16:09
26:29
Daia Reviewer..
11/11/96
Page 2 of2
X237 _PSR ll.U, LARS 61XM
Triangle Laboratories, inc.®
801 Capitals Drive » Durham, North Carolina 27713
Phone: (919) 544-5729 • Fax: (919) 544-5491
Printed: 16:0411/11/96
177
-------
TLI Project: 39291rl
Client Sample: 23B-1
Toxicity Equivalents Report
Analysis File: T966604
Client Project:
Sample Matrix:
TLI ID:
Sample Size:
Dry Weight:
GC Column:
Eastern Ridge Lime Facility
M23TRAIN Date Received: 10/19/96
143-23-4A,B Date Extracted: 10/21/96
Date Analyzed: 11/01/96
1.000 Dilution Factor: n/a
n/a Blank File: T966616
DB-5 Analyst: BB
Spike File:
ICal:
ConCal:
% Moisture:
% Lipid:
% Solids:
SPX23708
TF53286
T966598
n/a
n/a
n/a
2,3,7,8-TCDD
1,2,3,7,8-PeCDD
1,2,3,4,7,8-HxCDD
1,2,3,6,7,8-HxCDD
1,2,3,7,8,9-HxCDD
1,2,3,4,6,7,8-HpCDD
1,2,3,4,6,7,8,9-OCDD
TOTAL PCDD
2,3,7,8-TCDF
1,2,3,7,8-PeCDF
2,3,4,7,8-PeCDF
1,2,3,4,7,8-HxCDF
1,2,3,6,7,8-HxCDF
2,3,4,6,7,8-HxCDF
1,2,3,7,8,9-HxCDF
1,2,3,4,6,7,8-HpCDF
1,2,3,4,7,8,9-HpCDF
1,2,3,4,6,7,8,9-OCDF
TOTAL PCDF
0,01
0.02
0.02
0.02
0.02
0.05
0.34
0.04
0.02
0.03
0.04
0.02
0.02
0.02
0.07
0.01
0.06
x
x
X
X
X
X
X
X
X
X
X
X
X
X
X
X
X
1
0.5
0.1
0.1
0.1
0.01
0.001
0.1
0.05
0.5
0.1
0.1
0.1
0.1
0.01
0.01
0.001
0.01
0.01
0.002
0.002
0.002
0.0005
0.00034
0.0268
0.004
0.001
0.015
0.004
0.002
0.002
0.002
0.0007
0.0001
0.00006
0.0309
Total EPA TEFs, 1989a: 0.0577 ng
Page 1 of 1
TEFFRr5.OS.LARS6.fle.00
Triangle Laboratories, Inc.®
801 Capitola Drive • Durham, North Carolina 27713
Phone: (919) 544-5729 • Fax: (919) 544-5491
Printed: 16:21
11/11/961
-------
Initial ....Date...
Data Review By:
|C\/UJ _]_/_/JL/.22- Calculated Noise Area:
4.72
The Total Area for each peak with an ion abundance ratio outside
ratio limits has been recalculated according to method requirements.
Page No. 1
11/11/96
Compound/
M_Z.... QC.Log Omit Why
Listing of T966604B.dbf
Matched GC Peaks / Ratio / Ret. Time
.RT. OK Ratio Total.Area... Area.Peak.1.. Area.Peak.2.. Rel.RT Compound.Name.. ID.
TCDF
304-306
D
M
M
M
M
304-306
13C12-TCDF
316-318
DC NL 0:
13:
13:
13:
13:
14:
D cb 14 :
0.
00 RO
04
24
35
51
04
20
14:24
14:
14:
15:
15:
15:
16:
16:
38
59
11
25 RO
38
03
18
65-0.89
1.
0.
0.
0.
0.
0.
0.
0.
0.
0.
0.
0.
0.
0.
0.
13 Peaks
0.
DC NL 0:00
14:38 RO
15:11
15:35
16:03
DC WH 17:34
316-318
TCDD
320-322
38
80
67
71
82
82
72
88
81
74
80
96
78
70
80
1
5.
125.
75.
66.
311.
230.
70.
169.
142.
40
09
41
65
62
42
50
70
82
194.90
65.60
43.
37
185.96
48.
,45
21.18
55.
30.
27.
140.
103.
79.
63.
82.
29.
23.
81.
20.
9.
60
18
73
29
52
50
82
90
10
40
22
01
42
69.
45.
38.
171.
126.
0.828-1.138
49
23
92
33
90
90.20
79.
112.
36.
24.
104.
28.
11.
00
00
50
50
74
44
76
0.000
0.839
0.860
0.872
0.889
0.903
0.920
0.924
0.939
0.961
0.974
0.989
1.003 2378-TCDF AN
1.030
1.046
,681.17
65-0.89
0.78
0.51
0.71
0.74 8
0.78
0.83
4 Peaks
0.
DC NL 0:00 RO
14:01
D
D
M
M
D
320-322
14
DC SN 14
15
D SN 15
D SN 15
16
16
D SN 16
DC SN 16
DC WH 18
:20
:34 RO
:09
:24 RO
:48 RO
:09
:15
:23 RO
:49 RO
:04 RO
8
5,
38.
25
.72
.59
.98
,771.39
89.28
10
,925
fTV*TM
.01
.24
r> / rrv^'
.65-0.89
3
0
0
0
0
0
0
0
0
0
0
1
.64
.80
.69
.04
.72
.42
.32
.83
.80
.41
.28
.35
5 Peaks
1
99
47
0
49
6
3
14
24
6
1
0
235
.04
.24
.93
.53
.07
.92
.75
.91
.50
.48
.78
.76
.65
16.
10.
3,742.
39.
81
78
43
20
32.
15.
5,028.
50.
0.936-1.064
,89
,20
.96
,08
0.000
0.939
0.974
1.000 13C12 -2378-TCDF ISO
1.030
1.127
r\r\ Pi-il 1 i-iT TC
44.07
19.52
20.57
6
.77
10.90
55
0.
.17
28.41
28
8
13
.50
.14
.60
846-1.086
0.000
0.856
0.876
0.890
0.926
0.941
0.965
0.987
0.993
1.001 2378-TCDD AN
1.027
1.104
Triangle Laboratories, Inc.® Analytical Services Division
801 Caprtola Drive • Durham, North Carolina 27713
Phone: (919) 544-5729 • Fax: (919) 544-5491
Printed: 15:52 11/11/96
179
-------
Page No.
11/11/96
Listing of T966604B.dbf
Matched GC Peaks / Ratio / Ret, Time
Compound/
M_Z.... QC.Log Omit Why , .RT, OK Ratio Total .Area... Area. Peak. 1,. Area. Peak. 2.. Rel.RT Compound. Name.. IX>..
37C1-TCDD
328 DC NL
328 5
13C12-TCDD
332-334 DC NL
332-334 4
PeCDF
340-342 DC NL
M
DC SN
DC SN
DC SN
DC SN
DC SN
DC SN
DC SH
DC SN
D D SN
D D SN
A
M
M
A
DC SN
DC WH
DC WH
340-342 11
13C12 -PeCDF
352-354 DC NL
0:00
14:58
16:23
16:36
16:39
16:53
Peaks
0:00
15:10
16:09
16:22
16:47
Peaks
0.
18
18
18
18
18
18
19
19
19
19
19
20
20
20
20
20
20
21
21
21
22
22
23
23
:00
:00
:16
:31
:37
;42
:49
:04
:19
:28
:40
:54
:02
:09
:14
:28
:45
:51
:04
:15
:51
:00
:34
:20
-.21
0.
RO
1.
RO
RO
RO
RO
RO
RO
RO
RO
RO
RO
RO
RO
1.00
239.74 239.74
3,993.94 3,993.94
8.28 '8.28
4.09 4.09
7.07 7.07
4,253.12
65-0.89
2.66 3.88
0.75 31.57 13.58
0.81 4,744.44 2,117.35
0.79 7,642.69 3,362.68
0.72 73.59 30.71
12,492.29
17.
2,627
4,280
42,
32-1.78
0.42
1.63
2.68
0.58
0.45
0.18
0.50
3.29
0.75
1.43
1.63
1.48
1.47
1.22
1.65
1.52
0.95
1.37
1.49
1.46
1.61
1.62
0.20
1.75
0.56
Peaks
0
19
20
20
:00
:39
:24
:51
1,
RO
RO
.32-1.78
0.27
1.76
1.13
1.49
1
100
0
0
1
0
0
1
0
32
146
30
1
12
3
60
13
25
16
23
32
23
0
1
0
505
0
18
19
8,294
.02
.30
.64
.94
.43
.15
.89
.07
.76
.87
.23
.22
.78
.36
.60
.53
.93
.71
.71
.28
.07
.64
.34
.84
.77
.49
.41
.08
.06
.48
62
19
90
18
36
8
14
10
13
19
14
11
11
4,962
.10
.35
.55
.01
.54
.47
.85
.00
.80
.79
.60
.54
.59
.23
38
13
55
12
23
8
10
6
9
12
9
6
10
3,332
0.878-1.122
0.000
0.914
1.001 37C1-TCDD SUR1
1.014
1.017
1.032
0.878-1.122
0.000
.99 0.927
.09 0.987 13C12-1234-TCDD RSI
.01 1.000 13C12-2378-TCDD IS1
.88 1.025
0.855-1.112
.20
.52
.68
.21
.99
.96
.86
.71
.48
.28
.04
0.
.54
.25
.25
0.000
0.863
0.876
0.888
0.893
0.897
0.902
0.914
0.926
0.934
0.943
0.954
0.961
0.966
0.970
0.982
0.995
1.000 12378-PeCDF AN
1.010
1.019
1.048 23478-PeCDF AN
1.055
1.082
1.119
1.125
808-1.192
0.000
0.942
0.978
1.000 13C12-PeCDF 123 IS2
Triangle Laboratories, Inc.® Analytical Services Division
801 Capftola Drive • Durham, North Carolina 27713
Phone: (919) 544-5729 • Fax: (919) 544-5491
Printed: 15:52 11/11/96
130
-------
Page No.
11/11/96
Listing of T966604B.dbf
Matched GC Peaks / Ratio / Ret. Time
Compound/
M_Z.... QC.Log Omit Why ..RT. OK Ratio Total.Area... Area.Peak.1.. Area.Peak.2.. Rel.RT Compound.Name.. ID..
352-354
PeCDD
356-358
D
D
M
D
356-358
13C12 -PeCDD
368-370
6
21:15
21:50
23:00
Peaks
RO
RO
1.
1.
0.
18 32.35 19.68
51 4,647.90 2,797.68
57 4.69 2.86
13,016.56
1.32-1.78
DC
DC
DC
DC
DC
DC
D
D
DC
D
DC
DC
DC
DC
DC
DC
NL
SN
SN
SN
SN
SN
SN
SN
SN
SN
SN
SN
SN
SN
WH
4
NL
0:
19:
20:
20:
20:
20:
20:
20:
21:
21:
21:
21:
22:
22:
22:
00
54
21
26
32
37
42
56
09
21
39
55
08
20
30
22:40
22:52
23:03
23:23
RO
RO
RO
RO
RO
RO
RO
RO
RO
RO
RO
RO
RO
RO
1.
1.
4.
4.
1.
1.
3.
1.
1.
1.
1.
1.
0.
2.
0.
2.
27
14
73
64
56
59
36
50
02
56
53
28
78
12
27
07
1.23
2.
.31
0.71
Peaks
0:00
22:
1.
RO
f^e\_i^f / c^\~uu £• v^xxwwa
l.
45.
0.
0.
1.
1.
0.
33.
6.
20.
3.
14.
46
18 27.46
66
56
64
94
28
99 20.41
24
80 12.66
92
87 9.04
0.92
3.
0.
1.
1.
1,
1.
114.
52
.58
.73
.23
.38
.33
.84
32-1.78
8.20
:18 1.52
22:29
368-370
HxCDF
374-376
M
D
D
D
DC
DC
DC
DC
D
D
DC
D
DC
DC
SN
2
NL
SN
SN
SN
SN
SN
SN
SN
SN
22:40
RO
1.47
4
Peaks
0
24
24
24
24
24
24
24
25
25
25
25
25
:00
:07
-.16
:27
:31
:37
:48
:52
:14
:20
:26
:41
:44
1.
RO
RO
RO
RO
RO
RO
RO
RO
.18
It W«« . —
05-1.43
1
1
1
4
3
0
1
0
1
1
0
0
2
.32
.21
.28
.52
.82
.87
.60
.91
.27
.33
.70
.64
.68
0,
4,449
402
.13
.36 2,687.10
.08 239.14
2.42
16.65 1.
1,850.22 1'.
5.00 1.
019
047 13C12-PeCDF 234 SUR2
103
0.885-1.034
0.000
24.12 0.892
0.913
0,
0.
0.
0.
13.58 0,
0,
8.14 0.
0
7.04 0
0
1
1
1
1
1
1
.916
.921
.925
.928
.939
.948
.957
.971
.983
.993
.001 12378-PeCDD AN
.009
.016
.025
.034
.049
0.821-1.179
0
1,762.26 1
162.94 1
1
.000
.000 13C12-PeCDD 123 IS3
.008
.016
4,851.44
'• PoCDD / HxCDF Foil ows —
3
19
45
1
0
3
2
0
34
14
2
1
0
.13
.93 10.90
.83 25.72
.03
.38
.96
.93
.54
.33 19.23
.69 8.38
.42
.79
.85
0.945-1.064
0
9.03 0
20.11 0
0
0
0
0
0
15.10 0
6.31 1
1
1
1
.000
.952
.958
.965
.968
.972
.979
.982
.996 123478-HxCDF AN
.000 123678-HxCDF AN
.004
.014
.016
Triangle Laboratories, Inc.® Analytical Services Division
801 Capitola Drive • Durham, North Carolina 27713
Phone: (919) 544-5729 • Fax: (919) 544-5491
Printed: 15:52 11/11/96
131
-------
Page No.
11/11/96
Listing of T966604B.dbf
Matched GC Peaks / Ratio / Ret. Time
Compound/
M_Z.... QC.Log Omit Why ..RT. OK Ratio Total.Area... Area.Peak.1.. Area.Peak.2.. Rel.RT Compound.Name.. ID.
374-376
13C12-HXCDF
384-386
384-386
HxCDD
390-392
D
M
DC SN 25:52
25:56
DC SN 26:44
DC WH 26:59
5 Peaks
DC NL 0:00
24:07
24:16
25:13
25:20
25:55
26:06
26:40
7 Peaks
DC NL 0:00
D SN 24:45
25:15
DC SN 25:23
25:30
DC SN 25:55
DC SN 26:05
DC SN 26:23
DC SN 26:30
RO
RO
RO
0
RO
RO
RO
1
RO
RO
RO
RO
RO
RO
RO
2
1
0
1
.91
.32
.86
.67
0.76
13.02
0.90
0.34
127.80
7
.40
.43-0.59
1
0
0
0
0
0
0
0
.51
.30
.50
.48 3,
.48 5,
.49 3,
.63
.48 3,
15,
TkW^tm . U
1.27
10.43
12.89
244.39
763.60
543.14
3.37
007.99
585.81
rwir\r« /
.05-1.43
0
1
1
1
1
5
0
0
1
.94
.81
.23
.59
.12
.00
.25
.56
.51
2.84
3.02
113.65
0.72
11.98
0.74
1.36
0.40
1.50
3
4
1,057
1,880
1,164
1
979
.56
.28
.28
.79
.01
.41
.78
5.62
0.
11.70
8.61
2,187.11
3,882.81
2,379.13
2.23
2,028.21
1
1
1
1
.021
.024 234678-HxCDF
.055 123789-HXCDF
.065
AN
AN
842-1.158
0
0
0
0
1
1
1
1
.000
.952
.958
.995 13C12-HXCDF 478
.000 13C12-HXCDF 678
.023 13C12-HXCDF 234
.030
.053 13C12-HXCDF 789
SUR3
IS4
ALT2
ALT1
62
6
.75
.32
0.
50.90
5.66
939-1.017
0
0
0
0
0
0
0
1
1
.000
.946
.965
.970
.975
.990
.997 123478-HxCDD
.008
.013 123789-HxCDD
AN
AN
390-392
13C12-HxCDD
402-404
402-404
2 Peaks
125.63
1.05-1.43
0.962-1.038
DC NL
4
0:00 RC
25:30 RC
26:05
26:10
26:29
Peaks
3 1
3 2
1
1
1
.45
.34
.24
.23
.22
__ av«
2,
5,
3,
10,
•MTO . V
2
4
494
052
225
777
r-vnn
.30
.80
.34
.37
.78
.29
n / Hn
1,
2,
1,
fT\v T:
5.
381,
786.
774.
'ol 1,
.01
.50
.07
.51
1,
2,
1,
2
112
266
451
.14
.84
.30
.27
0.000
0.975
0.997
1.000
1.012
13C12 -HxCDD
13C12 -HxCDD
13C12-HXCDD
478 SUR4
678 IS5
789 RS2
HpCDF
408-410
M
M
M
DC
DC
DC
DC
DC
DC
NL
SN
SN
SN
WH
WH
0:00
28:18
28:33
28:42
28:46
29:25
29:33
29:43
29:55
30:03
0.88-1.20
RO 1.45
1.13
RO 1.36
RO 1.53
RO 0.31
RO
RO
RO
1
0
1
0
0
.62
.96
.44
.47
.93
1
63
8
9
0
1
5
0
0
1
.12
.65
.10
.91
.67
.06
.58
.65
.47
.33
0.995-1.051
0.000
33.76 29.89 1.000 1234678-HpCDF
5.40 3.97 1.009
7.46 4.86 1.014
1.016
1
2.74 2.84 1
1
1
1
.039
.044
.050
.057
.062
1234789-HpCDF
AN
AN
Triangle Laboratories, Inc.® Analytical Services Division
801 Capitola Drive • Durham, North Carolina 27713
Phone: (919) 544-5729 • Fax: (919) 544-5491
Printed: 15:52 11/11/96
132
-------
Page No.
11/11/96
Listing of T966604B.dbf
Matched GC Peaks / Ratio / Ret. Time
Compound/
M_Z QC.Log omit Why . .RT. OK Ratio Total,Area... Area.Peak.1.. Area.Peak.2.. Rel.HT Compound.Name.. ID..
408-410
13C12-HpCDF
418-420
418-420
HpCDD
424-426
4 Peaks
87.24
424-426
13C12-HpCDD
436-438
436-438
OCDF
442-444
442-444
OCDD
458-460
458-460
13C12-OCDD
470-472
470-472
DC
DC
DC
DC
DC
DC
DC
DC
DC
DC
DC
DC
DC
NL 0:00
28:18
29:33
29:48
29:50
4 Peaks
NL 0:00
SN 28:28
28:36
SN 28:44
SN 28:57
SN 29:01
SN 29:05
29:14
WH 29:37
2 Peaks
NL 0:00
28:36
29:14
29:26
3 Peaks
NL 0 : 00
31:46
SN 32:37
1 Peak
NL 0:00
31:43
1 Peak
NL 0 : 00
31:42
1 Peak
0.37-0.51
RO 0.87
0.43
0.44
0.44
RO 0.89
0.88-1.20
RO 1.54
RO 2.21
1.01
RO 4.68
RO 0.28
0.91
RO 1.53
1.02
1.14
0.88-1.20
RO 1.92
RO 0.86
1.04
1.11
0.76-1.02
0.80
0.88
RO 1.96
0.76-1.02
RO 0 . 09
0.92
0.76-1.02
RO 0 . 67
0.83
3.23
4,322.28
1,881.80
7.02
4.24
6,215.34
HpCDF /
1.10
0.96
18.90
0.45
0.63
1.26
0.81
25.03
2.23
43.93
2.31
9.50
4,189.02
7.20
4,205.72
; HpCDD /
2.48
25.71
0.91
25.71
0.08
116.74
116.74
0.04
5,367.50
5,367.50
1,301.51
576.45
2.13
2.63
Follows
9.52
12.65
4.85
2,132.66
3.79
0.929-1.141
0.000
3,020.77 1.000 13C12-HpCDF 678 IS6
1,305.35 1.044 13C12-HpCDF 789 SUR5
4.89 1.053
2.94 1.054
0.973-1.006
0.000
0.974
9.38 0.978
0.983
0.990
0.993
0.995
12.38 1.000 1234678-HpCDD AN
1.013
0.966-1.034
0.000
S.63 0.978
2,056.36 1.000 13C12-HpCDD 678 IS"!
3.41 1.007
Octa-CDD and CDF Follows
0.874-1.126
0.000
12.07 13.64 1.002 OCDF
1.029
0.874-1.126
0.000
55.87 60.87 1.001 OCDD
0.995-1.006
0.000
2,436.95 2,930.55 1.000 13C12-OCDD
AN
AN
IS8
Triangle Laboratories, Inc.® Analytical Services Division
801 Capitola Drive « Durham, North Carolina 27713
Phone: (919) 544-5729 • Fax: (919) 544-5491
Printed: 15:52 11/11/96
133
-------
Page No.
11/11/96
Listing of T9fi6604B.db£
Hatched GC Peaks / Ratio / Eat. Time
Compound/
M_Z.... QC.Log Omit Why ..BT. OK Ratio Total.Area— Area.Peak.1.. Area.Peak.2,. Rel.ET Compound.Name.. ID.
Column Description.
"Why" Code Description QC Log Desc.
M_Z -Nominal Ion Mass(es)
. .ET. -Retention Time {mnt:ss)
Rat.l -Ratio of M/M+2 Ions
OK -RO=Ratio Outside Limits
Rel.RT-Relative Retention Time
*** End of Report ***
WL-Below Retention Time window
WH-Above Retention Time Window
SN-Below Signal to Noise Level
-------
File:T966604 #1-835 Acq:l-NOV-96 00:20:57 EI+ Voltage SIR 70T
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315.9419 F:2 BSUB(356,30,-3.0) PKD(5, 3,1, 0 .101,5000.0,0 .00lrF,F) Exp-.EPCUS
TRIANGLE LABS Teit:23B-l TLI&39291X1 ItKT. TIME = 00:24
lOOJt JJ . 74E7
sol
40:
201
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100J
sol
60l
40,
20:
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13:00 14:00 15:00 16sOO 17:00
File:T966604 #1-835 Acq:l-NOV-96 00:20:57 EI+ Voltage SIR 70T Noise: 1608
317.9369 F:2 BSUB(256,30,-3 .0) PJOJf 5,3,1, 0.10%, 6432. 0, 0. 00%,F,T) Exp:EFCUS
TRIANGLE LABS Text'.23B-l TLI#39291R1 IJKT. TIME - 00 i:24
100* A5.03E7
802
sol
40:
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13:00 14:00 15:00 Iff.-OO 17:00
rile:T966604 #1-835 Acq:l-NOV-96 00:20:57 EI+ Voltaye SIR 70T
330.9792 F-.2 Exp:EPCUS
TRIANGLE LABS Text:23B-l TLI#39291R1 HOT. TIME = 00:24
l^J^-^J^^ 15£4^_r^_^5Ali--v-i?ll517:16
soJ
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13:00 14:00 15:00 Iff:00
File:T96SS04 #1-835 Acqsl-NOV-96 00:20:57 EI+ Voltagre SIS JOT
375.8364 F:2 Exp:EPC0S
TRIANGLE LABS Teit:23B-l TLI#39291Rl IKT. TIME
14:51
17:00
00:24
1003
80:
60:
40l
20:
0.
17:07
15:55
13:16
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1.1.2E5
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18:00 Time
3.9E5
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L5. 3E6
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18:00 Time
1.2S7
'-.9.6E6
-7.2E6
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18s 00 Time
17:53
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18:00
17:34
16:17
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-4.1ZJ
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13:00
14:00
15:00
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17s 00
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ISsOO Time
136
-------
Tile:T9666Q4 #1-835 Acqsl-SOV-96 00:20:57 EH- Voltage SIS 70T Soise:1073
319.8965 JT»2 BSUB{256,30, -3.0) fKS(5, 3,1,0 .10\,4292.0,0,QQ*,r,f) ExpsEPCUS
TRIANGLE LABS Texti23S-l TLIt39291MJ. MET. TIME » 00:24
100%
so:
sol
•
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FileiT966604 #1-835 Acqsl-KOV-96 00s20:57 EH- Voltage SIR 70T noise: 296
321.8936 T:2 BSUS( 256,30, -3 . 0) PKD(5, 3,1, 0.101,1184 .0, 0.00\,V,T) ExpsEPCOS
TRIANGLE LABS Text:23B-l TLI#39291M1 IXKT. TIME - 00:24
1004
so:
60.
40.
20.
Q-
R5.52E5
1
A2.84E5
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File:T966604 #1-835 Acq: l-KOV-96 00:20:57 EI+ Voltage SIS 70T Noise:2913
331.9368 F:2 BSUB(256, 30, -3.0) VU>( 5, 3,1, 0 .10%,11652. 0, 0. 00%, F,F) Exp-.EPCOS
TRIANGLE LABS Texts23B~l TLI#39291X1 HKT. TIME = 00:24
1001
80:
sol
40:
20:
o:
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A
ft
A2.12E7
A
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14:00 15s 00 ' ' ' 16s 00 17:00 ' 18:00 Time
File:T966604 #1-835 Acq: l-KOV-96 00:20:57 El* Voltage SIS 70T Noise:1094
333.9338 F:2 BSUB(256, 30, -3. 0) FKD(5,3,1, 0.101,4376. 0,0. QO*,F,F) Exp-.EFCVS
TRIANGLE LABS Texts 23S-1 TLIH39291R1 IMJ. TIME « 00:24
1003
80:
•
602
40!
20:
o-
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A
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F±lesT9SS604 #1-835 Acg:l-NOV-96 00:20:57 EH- Voltage SIS 70T noise: 502
327.8847 Ft 2 BSOB( 256,30, -3. 0) PKD(5,3,1, 0.101,2008. 0, 0. OOl,F,F) ExpsEPCUS
TRIANGLE LABS Text:23B-l TLI#39291X1 IJTJ". TIME - 00 .-24
100J
80.
60.
40.
20.
0
A3 . 99E7
A
A
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8.5E6
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14sOO ' ISiOO ISsOO 17:00 isloo Time
File:T968604 #1-835 Acg:l-NDV-96 00:20:57 EH- Voltage SIS 70T
330.9792 Fs2 ExpiEfCtfS
TRIANGLE LABS Text:23B-l TLI#39291X1 IJKT, TIME - 00:24
100S
80.
60,
40,
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0.
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FilesT966604 #1-835 Acqsl-SOV-96 00:20:57 EI+ Voltage SIS 70T JToiaesJOfl
339.8597 F-.2 MSUB(256,30, -3. 0) PKD(5, 3,1,0. 10%,1232. 0,0. 00*,f,r; Exp:EPCUS
TRIANGLE LABS Text:23B-l TLI#39291S1
1003
aol
sol
•
40:
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201
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FilesT9S6S04 #1-835 Acq:l-JK>V-96 00:20:57 EH- Voltage SIS 70T JToiae: 74 7
341.8567 Fs2 BSUB{ 256, 30, -3. 0) PKD( 5, 3,1, 0.10^,2988. 0,0, 00%, F,F) Sxp:EPCUS
TRIANGLE LABS Text:23B-l TLH39291S1
1003
aol
sol
401
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-2.3E4
21:00 22:00 23:00 Time
File:T966604 #1-835 Acq:l-NOV-96 00:20:57 EI+ Voltage SIS 70T Noiaesl25
351.9000 F:2 BSO3(256,3Q, -3.0) PKD(S,3,1, 0.10%, 500.0, 0
TRIANGLE LABS Texts 23B-1 TLIK3S291S1
1003
sol
"
601
401
201
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'la's oo
' 19s 00
A4.
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'20.' oo'
File:T966604 #1-835 Acq:l-NOV-96 00:20:57 EH- Voltage
353.8970 F:2 BSUB(256, 30, -3. 0) PKD( 5, 3,1, 0.101,1844. 0,
TRIANGLE LABS Text:23B-l TLI#392$1X1
1003
aol
601
401
201
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'ia\oo'
'l5:0o'
^3.
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'20:00'
F±lesT9SS604 #1-835 Acqsl-KOV-96 00:20:57 EH- Voltagre
330.9792 F:2 Exp:
EPCUS
TRIANGLE LABS Text:23B-l TLH39291S1
1003
aol
601
401
201
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t IB til 18
•^ V*M- \/~
'is-oo'
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17KT. TIME = OOs 24
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.
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19.2E6
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SIS 70T Noise: 461
Q.OO%rF,F) Exp: EPCUS
JKT. TIME = 00:24
33E7 7.8E6
A1.8SE7
A
ft
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21-00' ' ' '22:00 23sOo' ' ' Time
SIS 70T
IJKT. TIME = 00:24
IS:46 20:42 21:10 21:56 22:30
'20»00'
File:T96S604 #1-835 Acqsl-NOV-96 00:20:57 EI+ Voltage
409.7974 Ft 2 Exp:
EPCUS
TRIANGLE LABS Texts 23B-1 TLI #39291X1
1003
sol
601
401
201
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"—i 1 1 1 i—
18s53
t
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19:00
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SIS 70T
UKT. TIME " 00:24
C1.5E4
20:59
i
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l/Lj^JJ^LJA^^
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-8.8E3
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21 .-00 22 .-00 23:00 Time
133
-------
20:00 21:00 22:00
File:T966604 #1-835 Acq:l-NOV-96 00i20:57 Elf Voltage SIS 70T NoiaetSSO
357.3516 F:2 BSUB(2S6,30, -3.0) PKD(S,3,1, 0.10%,1400. 0,0,00%,F,F) Exp:EPCUS
TRIANGLE LABS Text:23B-l TLI#39291X1 JKT. TIME - 00:24
100S.S2.41E5
so:
Ue:TSS$604 #1-63
55.8545 F:2 BSU3(2$6,30, -3.0) J>JOJf5,3,l,0.10%,1775.0,0.00%,J>',i'j ExptEPCOS
TRIANGLE LABS Teit:23B-l TLI#39291R1 JWT. TIME - 00:24
00* *2. 75*5
23:00
20:00 21:00 22:00
JTile:T966604 #1-835 Acq:l-iTOV-96 00:20:57 EI+ Voltage SIR 70T Noise:205
367.8949 F:2 BSUB(2S6,30r -3.0) PKD(5,3,1, 0.10%, 820 .0, 0. 00%,F,F> ExpsEPCUS
TRIANGLE LABS Text.-23.B-l TLI#39291X1 IJW. TIME = 00:24
1004 . A2.69E7
so
so:
20:
23:00
20:00 21:00 22:00
File:T966604 #1-835 Acq:l-NOV-96 00:20:57 EI+ Voltage SIR 70T Noise:23
3S9.8919 F:2 BSUB(256,30, -3. 0) PJOJf5,3,l, 0.10%,S2.0, Q.OQ\,F,F) ExpsEPCUS
TRIANGLE LABS Text:233-1 TLI#39291S1 IKT. TIME = 00:24
1003,
so:
so:
40:
20:
23:00
I . S3E6
20:00 21:00 22s00
File:T9S6604 #1-835 Acq:l-NOV-9S 00:20:57 EI+ Voltage SIX 70T
330.9792 F:2 ExpiEfCPS
TSIAKSLE LABS Text:23B-l TLI#39291S1 IlfJ". TIME - 00:24
"^-SSA^i^wwW2^ .^^_22:1722:30
80J
eo:
40:
20.
0.
23:00
Time
rS.6ES
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12.6E6
11. 3ES
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-1. 8£6
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20:00
21:00
22: 00
23:00
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Timi
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-------
FileiTS66604 #1-505 Acq:l-NOV-96 00:20:57 SI+ Voltage SIS 702" KoisesBBB
373.8208 Fi3 BSUB(2S6, 30, -3. 0) PKD(5,3,1, 0.10%,3552. 0,0. 00*,F, f) ExpiEPCUS
TRIANGLE LABS Texti23B-l TLX#39291M1 IHJT. TIME - 00:24
1003k A2.57E5
24:00 25:00 26:00
TiletT966604 #1-505 Acqil-NOV-36 00i20s57 EI+ Voltage SZS 70T No±ae:674
375.8178 Fs3 BSUS(256, 30, - 3. 0) PXD(5, 3,1, 0.101,2696. 0,0.00%, J*,?) EipiEPCUS
TRIANGLE LABS Text:23B-l TLI#39291R1 I«T. TIME = 00:24
1004 A2.Q1E5
24:00 25:00 26:00
Fil«:T966604 #1-505 Acqtl-NOV-96 00:20:57 EI+ Voltage SIR 70T Noise:636
383,8639 F:3 BSUB(256,30, -3.0) PKD(5,3,1,0.10%,2544.0,0.00%,JP,F,> Exp-.EPCUS
TRIANGLE LASS Text:23S-l TLI#39291S1 I2KT. TIME - 00:24
1001 A1.88E7
27:00
80.
601
401
201
01
A1.51E5
A8.30M4
AS.62E4
A2.52E4
7.48E3 h A1.31E4
A2.23E3
A9.88E3
27:00
80:
60:
401
201
A1.16E7
A9.SOE6
24:00 25:00 26:00
File:T966604 #1-505 Acq:l-NOV-96 00:20:57 EI+ Voltage SIR 70T Noise:419
385.8610 Fs3 BSVS(256,30,-3 .0) PKD( 5, 3,1, 0.10%, 1676.0, 0.00*,F,f) Exp:EPCUS
TRIANGLE LASS Text:23B-l TLH39291R1 1X3". TIME = 00:24
IOCS A3.88E7
27:00
eo:
40:
20:
o.
A2.38E7
A2.03E7
24:00 25:00 26:00
File:T966604 #1-505 Aoqsl-NOV-96 00:20:57 EI+ Voltage SIR 70T
392.9760 F:3 Exp:EPCUS
TRIANGLE LABS Text:23B-l
100%, 24:34
80:
60:
40:
20:
o":
TLI#39291R1
24 i 51 25:0925:21
IWJ. TIME
25:52 26:07
27:00
00:24
26:31 26:47 27:00
24:00 25:00 26:00
F±lesT966604 #1-505 Actjsl-NOV-96 00:20:57 EI+ Voltage SIS JOT
445.7555 F:3 ExptSPCUS
TRIANGLE LABS Text:23B-l TLI#39291R1 INJT. TIME
25:17
27:00
.6.7T4
.5.4E4
.4.0E4
.2.7S4
.1.3E4
.O.OEO
Time
.5. 7E6
.4.6E6
.3. 4E6
.2. 3E6
.1. 1JE6
.O.OEO
TOJBE
.1.2E7
.S.2E6
.S.9E6
.4.6E6
.2.3E6
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Time
1.2JT7
.S.7E6
7.3E6
4.9E6
2.4E6
tt.OEO
Time
24 s 00
25:00
26:00
27:00
-------
tl-5'05 Ac?:l-ltoV-96 00:30:57tt+ Voltage SIS 7ST Xaiae: 765
83.8156 F:3 BSUS(256r30,-3.0) PgE(5,3,l, 0.10%, 3140.0,0,00%,!', t) ExpsEPCUS
TRIXHGLE JABS Teat: 23S-1 TLH39291M1 IK7. TIME - 00:24
00* A6.27E5
so:
601
401
24:36 24:48 25:00 25:12 25:24 25:35 25:48 26:00 26:12 26:24 26:36 26:48
lie .-ITS 66604 #1-505 Acq:l-«OV-S6 00:20:57 EI+ Voltagr* SIM 70T Koine;834
391.8127 F:3 BSUB(256,30,-3.0) J»KBf5,3,1,0.101,3.336.0,0.00%,F,.F,! ExpsEPCOS
TRIANGLE LABS Texts23B-l TLI#3929im JMT. TIME = 00:24
1003k AS. OSES
20.
A2.44S4
A6.0SS4
801
601
40.
201
A1.35E4
\
A4.16E4
A6.26E3
.S3.01JT4
. 65E3
24:36 24:48 25:00 25:12 25:24 25:36 25:48 26:00 26.-12 26:24 26:36 26:48
jrile:T966604 #1-505 Aeg-.-l-.WOV-.96 00:20:57 EI+ Voltage SIS 701 .Noise: 743
401.8558 F:3 BSVB(256r30, -3. 0) PKDf5,3,l, 0.10%,2S72.0,0. 00%,F,FJ Exp:EPCOS
TRIANGLE LABS Text:23B-l TLI#39291S1 JUST. TIME = 00:24
1003, A2.79E7
801
601
401
201
A1.38E
Al.77E7
24:36 24:48 25:00 25:12 25:24 25:36 25:48 26:00 26:12 26:24 26:36 26:48
Filc:rS66604 #1-505 Acq;l-NQV-96 00:20:57 EI+ Voltage SIS 70T iStoise.-515
403.8529 f:3 BSUB(25S, 30, -3. 0) FKD( 5,3,1, 0.10%, 2060. 0,0. 001,F,F) ExptEPCUS
TXIAffSLE LABS Texts23B-1 TLH39291S1 IKT. TIKE = 00:24
1004 . A2.27E?
801
601
401
201
Al.ll
A1.4SE7
24:36 24:48 25*00 25:12 25:24 25:36 25:48 26:00 26:12 26:24 26:36 26:48
Jfile:T966604 #1-505 Acq:l-NOV-9G OOi20iS7 EH- Voltage SIS 70T
392.9760 r:3 Exp:EPCtTS
TRIANGLE LABS Teoct:23B-l TLI039291S1 UKT. TIME 00:24
25:21 OS-11 25:57 26:07 26.1S 26:31 26:47
sol
60;
401
201
0.
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.1. 5E5
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Time
.1.4E5
.1.1E5
.8.6E4
.5.7E4
.2. 9E4
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Time
.S.5E6
.6.8E6
.5.1E6
.3,4E6
.1. 7E6
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Time
24:36 24:48 25.-00 25:12 25s24 2S.-36 25.-4S 26:00 26:12 26:24 26s36 2S.-48
.6.SE6
.5. 5E6
.4.1E6
.2.8E6
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Time
.1.2E7
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.4. 8E6
.2.4E6
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Time
-------
'ile:T96S604 #1-443 Acq:l-KOV-96 00.-20.-S7 EX+ Voltage SIR 70T Noiaes400
407,7818 F:4 MSUJB(256r30,-3.0) PKD( 5, 3,1, 0.10\, 1600 ,0,0, 00*, TfT) ExpiEPCUS
TRIANGLE LABS Text:23B-l TLI*39291S1 XKT. TIME - 00:24
100S A3.38E5
80:
eo:
40:
A2.14E4
28:12 28:24 28:36 28:48 29:00 29:12 29:24 29:36
File:T966604 #1-443 Acq:l-JfOV-96 00:20:57 EI+ Voltage SIS 70T lToise:277
409.7789 F:4 BSUB(256,30, -3.0) PKD(5,3,1, 0,101,1108. 0,0,OOl,F,F) Exp:EPCf}S
TRIANGLE LABS Text:23B-l TLI#39291R1 IJKT. TIME = 00:24
1003, A2.99E5
SO:
60:
28:12 28:24 28:36 28:48 29:00 29:12 29:24 29:36
File:T966604 #1-443 Acq:l-NOV-96 00:20:57 EI+ Voltage SIX 70T Noiae:976
417.8253 F:4 BSUB(256, 30, -3 . 0) PKD(5, 3,1, 0.10%, 3904. 0,0. 00%,7,F) ExpsEPCUS
TRIANGLE LABS Text:23B-l TLI#39291R1 IJW. TIME = 00:24
1001 A1.30E7
80:
60:
40: I \ A5.76E6
20":
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430.9729 F:4 Exp:EPCUS
TRIANGLE LABS Text:23B-l TLI#39291M1 IKT. TIME = 00:24
1004 28*2.3 28:30 28:54 29^05 29:13
29:48
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File:T966604 #1-443 Acq:l-KOV-96 00:20:57 EI+ Voltage SIS 70T
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29:24
29:36
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TRIANGLE LABS
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28:12
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28:36
28:40
29:00
29:12
29:24
29:36 29:48
30:00
132
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TRIANGLE LABS TtUCt:23B-l TLI#39291M1 1WJ. TIME = 00:24
004 A1.27E5
801
601
401
201
28:30 28:36 28:42 28:48 28:54 29:00 29:06 29:12 29:18 29:24 29:30 29':36
File:T966604 #1-443 Acqsl~NOV-9S 00:20:57 £1+ Voltage SIS 70T Xoiae:269
425.7737 F:4 BSUB(256,30, -3. 0) PKD(S,3,1,0.10*,1076.0,0.00*,F,F) Exp:EPCUS
TRIANGLE LABS Text:23B-l XLI#39291X1 XWJ. TIME - 00 -.24
1004 A1.24E5
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601
40.
201
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435.8169 F:4 SSUM(256,30,-3.0) PKD(5,3,1, 0.101,4344, 0,0, 00%, F, F) Exp:EPCUS
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437.8140 F:4 SStm(256,30, -3.0) FJOJfS, 3,1, 0,10\,2256.0,0.00\,F,F) Exp:EPCUS
TRIANGLE LABS Text:23B-l TLI#39291R1 IKT. TIME = 00:24
1001 A2.06E7
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430.9729 F:4 ExptEPCUS
TSIAOSLS LABS Text:23B-l TLI&39291S1 XKT. TIME = 00:24
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801
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TRIANGLE LABS Text:23B-l TLI#39291M1 I1KT. TIME - OOs 24
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513.6775 F:4 Exp:EPCUS
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-------
TLI Project: 39291rl
Client Sample: 23B-1
Method 23 TCDD/TCDF Analysis (DB-225)
Analysis File: X964236
Client Project:
Sample Matrix:
TLI ID:
Eastern Ridge Lime Facility
M23TRAIN Date Received: 10/19/96
143-23-4A,B Date Extracted: 10/21/96
Date Analyzed: 11/01/96
Spike File: SPC2NF08
ICal: XF21266
ConCal: X964226
Sample Size:
Dry Weight:
GC Column:
1.000
n/a
DB-225
Dilution Factor: n/a
Blank File: T966616
Analyst: JF
% Moisture: n/a
% Lipid: n/a
% Solids: n/a
2,3,7,8-TCDF
0.04
0.66
20:20
Internal Standard
Ami (ng)
% Recovery
QC limits
Ratio
RT
Flags
13C,r2,3,7,8-TCDF
6.6
82.4
40%-130%
0.78
20:21
13C12-1,2,3,4-TCDD
0.80
19:23
Data Reviewer
11/11/96
Page 1 of 1
C2NF.PSR ¥1.14, LARS 6.C8.00
Triangle Laboratories, Inc.®
801 Caprtola Drive • Durham, North Carolina 27713
Phone: (919) 544-5729 • Fax: (919) 544-5491
Printed: 16:1311/1
Iffl
-------
Initial
---- Date..
Data Review By:
Calculated Noise Area:
7,00
The Total Area for each peak with an ion abundance ratio outside
ratio limits has been recalculated according to method requirements.
Page No. 1
11/01/96
Compound/
M_Z.... QC.Log Omit Why
Listing of X964236B.dbf
Matched GC Peaks / Ratio / Ret. Time
..RT. OK Ratio Total.Area... Area.Peak.1.. Area.Peak.2.. Rel.RT Compound.Name.. ID.
TCDF
304-306
304-306
13C12-TCDF
316-318
316-318
13C12-TCDD
332-334
DC NL 0 : 00
16:10
17:07
17:30
17:45
17:54
18:02
18:10
18:21
18:40
19:06
19:20
19:31
19:43
19:50
20:13
20:20
20:32
20:42
20:53
21:27
DC WH 22:18
DC WH 22:28
20 Peaks
0.65-0.89
RO 0.37
0.
0.
RO 0.
RO 0.
0,
0.
0.
0.
0,
0,
0,
0,
RO 0.
0
RO 0.
0
0,
0
0
RO 1
RO 1
RO 0
.89
.83
,99
,91
,78
,88
.78
.69
,80
.79
.80
.70
.54
.79
.61
.66
.76
.80
.81
.16
.33
.36
3
8.
307.
227.
121,
136.
279.
82.
449.
223.
428.
179.
241.
148.
40.
153.
116,
120.
133.
69.
141.
29.
4.
2.
,630.
67
99
07
59
25
64
81
89
47
75
41
28
29
06
12
28
48
67
71
47
01
46
20
24
0.788-1.094
0.000
145
102
67
69
122
38
196
91
190
79
107
60
17
67
50
47
57
30
63
18
.30
.67
.99
.89
.38
.74
.75
.60
.73
,01
.19
.87
.53
.56
.34
.82
.90
.96
.25
.98
162.
124.
68.
77.
157.
44.
253.
131.
238.
100.
134.
87.
32.
85.
83.
72.
75.
38.
78.
16.
0.65-0.89
DC NL 0:00
DC WL 19:04
DC WL 19:20
20:21
20:50
DC WH 22:08
2 Peaks
RO 5
0
0
0
0
0
.89
.73
.71
.78 23
.65
.82
23
1.
81.
127.
,448,
232.
350.
,681.
33
53
57
30
86
00
.16
TCDF /
10,296
91
TCDD Folio
.50
.85
13,151,
141,
0.65-0.89
DC NL 0:00
19:12
19:23
DC SN 19:36
DC SN 19:44
20:02
RO 4
0
0
RO 2
RO 2
0
.05
.79 15
.80 10
.52
.29
.84
1.
,865.
,252,
,93
.78
.82
6,989
4,571
.26
.10
8,876
5,681
69
40
71
14
26
07
14
87
02
40
09
42
17
56
.17
66
.77
.75
,22
.42
0.
0.
0.
0.
0.
0.
0.
0.
0.
0.
0.
0.
0.
0.
0.
0.
1.
1.
1.
1.
1.
1.
794
841
860
872
880
886
893
902
917
939
950
959
969
975
993
999 2378-TCDF AN
009
017
026
054
096
104
0.951-1.049
.80
.01
0.
.52
.72
7.42
5,
,12
224.47
102
.52
121
.95
0.
0.
0.
1.
1.
1.
000
937
950
000 13C12-2378-TCDF ISO
024
088
896-1.104
0.
1.
1.
1.
1.
1.
000
000 13C12-2378-TCDD IS1
010 13C12-1234-TCDD BS1
021
,028
,043
Triangle Laboratories, Inc.® Analytical Services Division
801 Capftola Drive • Durham, North Carolina 27713
Phone: (919) 544-5729 • Fax: (919) 544-5491
Printed: 19:4411/01/96
212
-------
Page No. 2 Listing of X964236B.dl>f
11/01/96 Matched GC Peaks / Ratio / Ret. Time
Compound/
M_Z.... QC.Log Omit Why ,.RT. OK Ratio Total.Area... Area.Peak.1., Area.Peak.2.. Rel.RT Compound.Name.. ID.
DC WH 21:40 RO 2.43 11.24 1.128
332-334 3 Peaks 26,343.07
Column Description. "Why" Code Description QC Log Desc.
M_Z -Nominal Ion Mass(es) WL-Below Retention Time Window A-Peak Added
. ,RT. -Retention Time {min:ss} WH-Above Retention Time Window K-Peak Kept
Rat.l -Ratio of M/M+2 Ions SN-Below signal to Noise Level D-Peak Deleted
OK -RO=Ratio Outside Limits
-------
303,9016
Saaplm Text:
2009!
m-783 Aeg;
10tS4,Si SC BI+ Voltage
23B-1 TLI#39291rl Pile Text:TRIANGLE LABS
19:20
Auto£p*c
19:00 19:12 19:24 19:36 19:4B 20sOO 20:12 20:24
Flle:X96423S #1-783 Acg: l-NOV-1996 18:54:38 OC SI* Voltage SIR AutoSpoc
305.8987 Exp ! XCONP_TT
Saa?pl* Texts23B-l TLI#392Slrl File TeatttTRIAtKUJB LMBS
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214
-------
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100* A2.93SS
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315.9419 BSUBl25e,3Q,~3.Q) ?KD(5,3,1, 0.10*, fl8<8. 0, 0. 0000 19:00 20:00 21:00
Fil»:X9S4236 #1-783 Acqs l-NOV-1996 18*54*38 OC fil* Voltage SIR AutoSp»=
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100*
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9.7E4
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11. 9E7
.1.4E7
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-------
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ft 18:40
16:10 17:21 PI j 1S-20
I \ Iv 1 ft Jd A 1 1 1\ 1 19(t°6 1 n 1 2°i "
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.3.525
.2,325
.2.625
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00 17:00 ' ' ' 28:00 ' ' 15:00 ' 20:00 ' ' ' 21:00 ' 22:00 ' ' Time
:X964236 #2-783 Ac?: l-HOV-1996 18:54:38 OC 2X+ Voltage SIX AutoSpsc
S4I5 gaeptXeOBF^TT
le Text:23B-l TLI«39291rl File TextiTRIANOLE LABS
20:21 2.327
11
.1.527
.2.4E7
.5 . 426
.4.726
0.020
00 17:00 ISiOO 15:00 20:00 22:00 22:00 Time
SX964236 #1-783 Acgi l-KOV-1996 18:54:38 OC 21+ Voltage SIS AutoSpeo
8565 'S3fpsXCOOP_fT
la T«ort:23S-l TLI#39291rl File TaxttTRIAXOLE IASS
17 01 2.625
27:25
18:0818:31 25,20 ^^ ^^ ^^
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•00 ' ' 17*00 ' ' 28:00 ' ' ' 25:00 ' ' ' 20:00 ' ' ' 22:00 ' ' ' 22:00
•.X964236 #1-783 Acg: l-SOV-1996 18:54:38 OC 21+ Voltage SIR AutoSpec
9368 2xp:jTCOMF_W
1m Tmxt:23B-l TIiX#39291rl File TextiTKXANQLE IABS
19 1 12
|
Ivi
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1X964236 #1-783 Acgs 2-JWF-2SS6 18:54:38 OC JET* Voltage SIR AutoSpoa
5825 EXpsXCQNP_TT
le Text:23B-l TLI#39291rl Pile Text t TRIAKOLB ItABS
16-29 27:20 18:24 25:04 15:51 20:16 20J48 ^iSLj-w^
-f^^^~i*vv*^-*f^*ft«r~y<~~y"*^'Tf^l^^
tOO 27:00 18:00 15:00 20:00 21:00 22:00
HX964236 #1-783 Acgi l-SOV-1996 lBi54s38 OC 21+ Voltmge SIS AutoSpec
97 S 2 SxptXCOSF_TT
•>le Tmxts23B-l TLI#39291rl Pile Text.-TRIANQLE LABS
\ 16 24 16-52 17-17 28:37 25:22 20:00 20:31 %&2?^^^~^i£3*^+-
tOO 17»00 18:00 ' ' 25:00 ' ' 20»00 21800 ' ' 'a2iOO
12.225
12.625
" 0.020
Time
C1.4E7
.2.227
L8.226
If. 426
12.726
' 0. 020
5.827
17.527
L5.527
13 . 527
12.027
' 0.020
Time
8.827
.7.027
.5.327
.3.527
.2.827
0.020
217
-------
Peak Locate Examination: l-NOV-1996:18:54 File:X964236
Experiment:XCONF_TT Function:1 Reference:PFK
-------
TLI Project: 39291rl
Client Sample: 23B-2
Method 23 PCDD/PCDF Analysis (a)
Analysis File: T966605
Client Project:
Sample Matrix:
TLI ID:
Sample Size:
Dry Weight:
GC Column:
Eastern Ridge Lime Facility
M23TRAIN Date Received: 10/19/96
143-23-5A,B Date Extracted: 10/21/96
Date Analyzed: 11/01/96
1.000 Dilution Factor: n/a
n/a Blank File: T966616
DB-5 Analyst: BB
Spike File:
ICal:
ConCal:
% Moisture:
% Lipid:
% Solids:
SPX23708
TF53286
T966598
n/a
n/a
n/a
Analytes
2,3,7,8-TCDD
1,2,3,7,8-PeCDD
1,2,3,4,7,8-HxCDD
1,2,3,6,7,8-HxCDD
1,2,3,7,8,9-HxCDD
1,2,3,4,6,7,8-HpCDD
1,2,3,4,6,7,8,9-OCDD
Amt. (ng)
ND
ND
ND
ND
ND
0,03
EMPC
m, mt>& 8a&» mr Ffegs
0.01
0.02
0.02
0.02
0.02
0.95 29:14
0.09
2,3,7,8-TCDF
1,2,3,7,8-PeCDF
2,3,4,7,8-PeCDF
1,2,3,4,7,8-HxCDF
1,2,3,6,7,8-HxCDF
2,3,4,6,7,8-HxCDF
1,2,3,7,8,9-HxCDF
1,2,3,4,6,7,8-HpCDF
1,2,3,4,7,8,9-HpCDF
1,2,3,4,6,7,8,9-OCDF
0.07
ND
ND
0.02
0.006
ND
ND
EMPC
ND
EMPC
0.01
0.01
0.01
0.02
0.02
0.81
1.43
1.37
15:39
25:12
25:21
0.02
0.02
Total TCDD
Total PeCDD
Total HxCDD
Total HpCDD
Total TCDF
Total PeCDF
Total HxCDF
Total HpCDF
0.27
0.09
0.12
0.05
0.37
0.06
0.06
EMPC
5
3
1
2
2
5
0.15
0.13
0.54
0.02
Page 1 of2
X237J>SR vi.14, LKKS SMM
Triangle Laboratories, Inc.®
801 Captola Drive • Durham, North Carolina 27713
Phone: (919) 544-5729 • Fax: (919) 544-5491
Printed: 16:0511/11/9®
-------
TLI Project:
Client Sample:
39291rl
23B-2
Method 23 PCDD/PCDF Analysis (a)
Analysis File: T966605
BC,2-2,3,7,8-TCDF
13C,r2,3,7,8-TCDD
l3Ci2-l,2,3J,8-PeCDF
13C,2-l,2,3J,8-PeCDD
13C,2-l(2,3,6,7,8-HxCDF
13C12-l,2,3,6,7,8-HxCDD
I3C12-l,2,3A6,7,8-HpCDF
l3C,2-l,2,3,4,6,7,8-HpCDD
13C12-1,2,3,4,6,7,8,9-OCDD
6.1
6.2
6.0
5.5
6.3
6.9
6.6
6.6
9.4
76.5
78.0
74.4
68.8
78.9
86.1
82.1
82.0
58.8
40%-130%
40%-130%
40%-130%
40%-130%
40%-130%
40%-13Q%
25%-130%
25%-130%
25%-130%
0.74
0.79
1.56
1.50
0.49
1.24
0.43
1.03
0.84
15:36
16:23
20:51
22:18
25:20
26:11
28:18
29:14
31:43
37Cl4-2,3,7,8-TCDD
13C12-2,3,4,7,8-PeCDF
13Ci2-l,2,3,4,7,8-HxCDF
13Ci2-l,2,3,4,7,8-HxCDD
13C,2-l,2>3,4,7,8,9-HpCDF
4.3
4.0
4.8
4.4
4.3
107
101
119
110
106
70%-140%
70%-140%
70%-140%
70%-140%
70%-140%
1.47
0.49
1.24
0.44
16:24
21:51
25:13
26:05
29:34
13C!2-l,2,3,7,8,9-HxCDF
13C,2-2,3,4,6,7,8-HxCDF
3.8
3.7
93.9
91.6
40%-130%
40%-130%
0.49
0.48
26:40
25:55
13e,2-l,2,3,4-TCDD
13C)2-l,2,3,7,8,9-HxCDD
0.79
1.24
16:10
26:29
Data Reviewer
11/11/96
Page 2 of 2
X237_PSRvl.l4.LARS«.08.00
Triangle Laboratories, Inc.®
801 Capitola Drive • Durham, North Carolina 27713
Phone: (919) 544-5729 • Fax: (919) 544-5491
Printed: 16:05
9 .-,
-------
TLI Project:
Client Sample:
39291rl
23B-2
Toxicity Equivalents Report
Analysis File: T966605
Client Project:
Sample Matrix:
TLI ID:
Sample Size:
Dry Weight:
GC Column:
Eastern Ridge Lime Facility
M23TRAIN Date Received: 10/19/96
143-23-5A,B Date Extracted: 10/21/96
Date Analyzed: 11/01/96
1.000 Dilution Factor: n/a
n/a Blank File: T966616
DB-5 Analyst: BB
Spike File:
ICal:
ConCal:
% Moisture:
% Lipid:
% Solids:
SPX23708
TF53286
T966598
n/a
n/a
n/a
2,3,7,8-TCDD
1,2,3,7,8-PeCDD
1,2,3,4,7,8-HxCDD
1,2,3,6,7,8-HxCDD
1,2,3,7,8,9-HxCDD
1,2,3,4,6,7,8-HpCDD
1,2,3,4,6,7,8,9-OCDD
TOTAL PCDD
2,3,7,8-TCDF
1,2,3,7,8-PeCDF
2,3,4,7,8-PeCDF
1,2,3,4,7,8-HxCDF
1,2,3,6,7,8-HxCDF
2,3,4,6,7,8-HxCDF
1,2,3,7,8,9-HxCDF
1,2,3,4,6,7,8-HpCDF
1,2,3,4,7,8,9-HpCDF
1,2,3,4,6,7,8,9-OCDF
TOTAL PCDF
0.01
0.02
0.02
0.02
0.02
0.03
0.09
0.02
0.01
0.01
0.02
0.006
0.01
0.02
0.02
0.02
0.02
x
x
X
X
X
X
X
X
X
X
X
X
X
X
X
X
X
1
0.5
0.1
0.1
0.1
0.01
0.001
0.1
0.05
0.5
0.1
0.1
0.1
0.1
0.01
0,01
0.001
0.01
0.01
•0.002
0.002
0.002
0.0003
0.00009
0.0264
0.002
0.0005
0.005
0.002
0.0006
0.001
0.002
0.0002
0.0002
0.00002
0.0135
Total EPA TEFs, 1989a: 0,0399 ng
Page 1 of 1
TEFPR V5.08. LARS 6.« 00
Triangle Laboratories, lnc.«
801 Capitola Drive * Durham, North Carolina 27713
Phone: (919) 544-5729 • Fax: (919) 544-5491
Printed: 16:22 11/11/96
Oo 1
-------
Initial ....Date
Data Review By:
fCukJ _U_/_£L/2s. Calculated Noise
Area:
4.20
The Total Area for each peak with an ion abundance ratio outside
ratio limits has been recalculated according to method requirements.
Page No. 1
11/11/96
Compound/
M_Z.... QC.Log Omit Why
Listing of T966605B.dbf
Matched GC Peaks / Ratio / Ret.
Time
.RT. OK Ratio Total.Area... Area.Peak.1.. Area.Peak.2.. Rel.RT Compound,Name.. IB.
TCDF
304-306
M
D
M
M
M
M
304-306
13C12-TCDF
316-318
316-318
TCDD
320-322
D
M
M
D
320-322
DC NL 0:00
13:05
13:25
13:36
13:51
14:04
14:25
14:38
D cb 14:55
15:00
15:11
DC SN 15:20
15:26
15:39
16:04
16:18
13 Peaks
DC NL 0:00
14:38
15:11
15:36
16:03
DC WH 17:35
4 Peaks
DC NL 0:00
14:02
14:20
DC SN 14:59
15:11
D SN 15:27
DC SN 15:36
DC SN 15:51
16:10
16:17
D SN 16:24
5 Peaks
0.
65-0.89
0.
0.
,80
,79
0.74
0.75
RO
RO
RO
RO
RO
RO
RO
0.
RO
RO
RO
0,
RO
RO
RO
RO
RO
0,
0,
0,
0,
1,
0,
0,
0,
0
0,
1
0
65-
0
0
1
0
0
1
.82
.80
.55
.80
.68
.93
.99
.53
.86
.81
.12
.47
-0.89
.50
.66
.02
.74 8
.76
.01
8
4.
38.
21.
17.
106.
85.
49.
54.
24.
92.
29.
1.
65
41
89
40
26
37
19
25
66
04
91
59
24.40
82.
18.
7,
628,
2,
52,
18,
,602
84,
6.
,758,
nviTM
.65-0.89
1
0
0
5
0
0
4
0
0
0
0
,77
.77
.79
.42
.77
.86
.08
.41
.76
.66
.53
1
158
74
0
31
4
1
1
13
18
6
296
50
,94
,81
.37
.62
.49
.42
.87
.99
.84
.77
j / try*"1
" / i.\.
.59
.83
.74
,34
.51
.15
.17
.38
.23
.44
.18
.75
16.
9.
7.
47.
37.
21.
24.
48.
16.
11.
36.
12.
3.
20,
10.
3,652.
36.
98
29
47
98
90
40
18
50
70
30
98
00
38
87
62
36
78
21
12
9
58
47
38
30
52
16
13
45
10
7
31
10
4,950
48
0.828-1.138
.43
.60
.93
.28
.47
.90
.07
.00
.90
.10
.52
.70
.25
0.
.62
.40
.51
.21
0.000
0.839
0.860
0.872
0.888
0.902
0.924
0.938
0.956
0.962
0.973
0.983
0.989
1.003 2378-TCDF AN
1.030
1.045
936-1.064
0.000
0.938
0.973
1.000 13C12-2378-TCDF ISO
1.029
1.127
69.
33,
13.
32
,08
.73
5.70
7.31 -
89
41
17
7
11
0.
.51
.66
.78
.53
.13
846-1.086
0.000
0.857
0.875
0.915
0.927
0.943
0.952
0.967
0.987
0.994
1.001 2378-TCDD fiN
Triangle Laboratories, Inc.® Analytical Services Division
801 Capftola Drive » Durham, North Carolina 27713
Phone: (919) 544-5729 • Fax: (919) 544-5491
Printed: 15:5311/11/96
2 '•' 2
-------
Page Ho.
11/11/96
Listing of T966605B.db£
Matched GC Peaks / Ratio / Ret, Time
Compound/
M_Z.... QC.Log Omit Why ..RT, OK Ratio Total.Area... Area.Peak,1.. Area.Peak.2,, Rel.RT Compound.Name.. ID..
37C1-TCDD
328
328
13C12-TCDD
332-334
DC NL 0:00
14:59
16:24
16:54
DC SN 17:35
17:46
4 Peaks
DC NL 0 : 00
15:10
0.
RO
RO
16:10
16:23
16:47
332-334
PeCDF
340-342
3,
3,
0.68
42.44 42.44
627.37 3,627.37
1.84 1.84
0.91
1.61 1.61
673.26
65-0.89
2.
1.
0.
0.
0.
4 Peaks
DC NL 0 : 00
1.
RO
18:01
DC SN 18:16
DC SN 18:48
DC SN 19:21
DC SN 19:29
D
D
340-342
13C12-PeCDF
352-354
352-354
PeCDD
356-358
19
DC SN 19
DC SN 20
DC SN 20
DC SN 21
D SN 21
D SN 22
DC SN 22
DC SN 22
:42
:56
:10
:39
:19
:52
:03
:12
:16
RO
RO
RO
RO
RO
RO
RO
RO
RO
RO
RO
RO
50
13
79 4,
79 7,
74
11,
4.
,32
24.19 15.44
441.35 1,964.74
270.94 3,207.78
80,
.22 34.08
0.878-1.122
0.000
0.915
1.001 37C1-TCDD
1.032
1.073
1.084
SOR1
0.878-1.122
13.67
2,476.61
4,063.16
46,14
0.
0.
0,
.000
.926
.987 13C12-1234-TCDD
1.000 13C12-2378-TCDD
1,
.024
RSI
IS1
816.70
32-1.78
0.
1.
1.
0.
0.
5.
1.
S.
4.
0.
4.
1.
0.
1.
5.
24
65
08
36
34
39
66
23
18
45
87
93
94
05
10
2 Peaks
DC NL 0
19
20
20
21
21
21
:00
:39
:24
1.
RO
RO
0.855-1.112
0.66
25.
.97 16.17
9.80
0.92
0
0
3
42
2
2
0
3
7
5
0
0
68
.80
.26
.06
.79 26.72
.91
.22
.51
.03
.91
.87
.95
.54
.76
32-1.78
0,
1,
,05
,77
1.11
:51 1.56 7
:04
$15
RO
RO
1.28
1,
.13
:51 1.47 4
6 Peaks
DC NL 0
19
:00
:55
1.
RO
RO
12
.32-1.78
2
1
.65
.27
0
27
14
,981
28
11
,091
.08
.96 17.88
.65 8.91
.44 4,861.77
.23 17.16
.29 6.85
.10 2,437.12
16.07
0.
10.08
8.02
3,119.67
13.41
6.08
1,653.98
0
0
0
0
0
0
0
0
0
0
1
1
1
1
1
.000
.864
.876
.902
.928
.934
.945
.956
.967
.990
.022
.049 23478-PeCDF
.058
.065
.068
AN
808-1.192
0
0
0
1
1
1
1
.000
.942
.978
.000 13C12-P6CDF 123
.010
.019
.048 13C12-PeCDF 234
IS2
SOR2
,154.67
0
41
.87
.47 25.21
0.
19.79
885-1.034
0
0
.000
.893
Triangle Laboratories, Inc.® Analytical Services Division
801 Capitola Drive « Durham, North Carolina 27713
Phone: (919) 544-5729 • Fax: (919) 544-5491
Printed: 15:5311/11/96
99
-------
Page No.
11/11/96
Listing of T966605B.dbf
Matched GC Peaks / Ratio / Ret. Time
Compound/
M_Z.,,. DC.Log Omit Why ..RT. OK Ratio Total,Area,.. Area.Paak.1.. Area.Peak.2.. Rel.RT Compound.Hame., ID,
356-358
13C12-PeCDD
368-370
368-370
HxCDF
374-376
M
MN
NM
374-376
13C12-HXCDF
384-386
384-386
DC
D
DC
D
DC
D
DC
DC
DC
DC
DC
DC
DC
DC
DC
DC
DC
DC
DC
DC
SN
SN
SN
SN
SN
SN
SN
WH
WH
WH
WH
4
HI.
3
NL
SN
SN
SN
SN
SN
5
NL
SN
6
20:31
20:55
21:07
21:20
21:28
21:39
21:56
22:07
22:19
22:54
23:05
23:11
23:15
23:25
Peaks
0:00
22:18
22:29
22:51
Peaks
0:00
24:07
24:17
24:38
25:12
25:21
25:34
25:57
26:16
26:44
26:52
Peaks
0:00
24:06
24:15
25:13
25:20
25:32
25:55
26:40
Peaks
RO
RO
RO
RO
RO
RO
RO
RO
RO
1.
RO
RO
1.
RO
RO
RO
RO
RO
0.
RO
RO
1.
1.
1.
1.
2.
1.
1.
0.
2.
0.
3.
1.
0.
1.
14
70
29
62
02
59
66
50
00
61
44
00
98
76
1
32
4
18
1
4
9
1
3
0
0
0
0
1
103
.45
.87 20.68
.47
.97 11.74
.35
.55
.83 6.13
,22
.70
.90
.64
.53
.99
.05
.14
32-1.78
12.
1.
1.
0.
25
50
53
91
05-1.43
0.
1.
1.
0.
1.
1.
0.
1.
1.
1.
0.
93
18
20
19
43
37
31
10
04
10
89
0
4,329
396
4
4,731
.10
.91 2,594.81
.80 239.82
.40 2.67
.11
12.19
7.23
3.70
0
0
0
0
0
0
0
0
1
1
1
1
1
1
.920
.938
.947
.957
.963
.971
.984
.992
.001 12378-PeCDD
.027
.015
.040
.043
.050
AN
0.821-1.179
1,735.10
156.98
2.94
0
1
1
1
.000
.000 13C12-PeCDD 123
.008
.025
IS3
2
7
13
0
12
5
.15
.73 4.18
.44 7.33 '
.34
.95 7.62
.54 3.20
0.945-1.064
3.55
6.11
5.33
2.34
. 0.20
9
0
0
0
49
.43 4.95
.49
.82
.31
.09
43-0.59
0.
0.
0.
0.
0.
0.
98
44
56
49
49
39
0.48
0.49
1
17
14
3,042
5,486
3
3,022
2,520
14,103
, . WvCT!
.57
.25 5.29
.92 5.36
.11 999.18
.38 1,792.97
.69
.52 982.94
.17 823.46
.35
iTP / TSEvfTyr^ t?i">1 T /"lure — —
4.48
0.
11.96
9.56
2,042.93
3,693.41
2,039.58
1,696.71
0
0
0
0
0
1
1
1
1
1
1
842
0
0
0
0
1
1
1
1
.000
.952
.959
.972
.995 123478-HxCDF
.001 123678-HxCDF
.009
.024
.037
.055 123789-HxCDF
,061
-1.158
.000
.951
.957
.995 13C12-HXCDF 478
.000 13C12 -HxCDF 678
.008
.023 13C12 -HxCDF 234
.053 13C12-HXCDF 789
AN
AN
AN
S0R3
IS4
ALT2
ALT1
Triangle Laboratories, Inc.® Analytical Services Division
801 Capitola Drive • Durham, North Carolina 27713
Phone: (i19) 544-5729 • Fax; (919) 544-5491
Printed: 15:5311/11/96
224
-------
Page No.
11/11/96
Listing of T966605B.dbf
Matched GC Peaks / Ratio / Ret. Time
Compound/
M_Z.... QC.Log Omit Why ..RT. OK Ratio Total.Area... Area.Peak.1.. Area.Peak.2.. Rel.RT Compound.Name.. ID.
HxCDD
390-392
390-392
13C12-HXCDD
402-404
402-404
HpCDF
408-410
408-410
13C12-HpCDF
418-420
418-420
1.05-1.43
DC
D
DC
DC
DC
DC
DC
DC
DC
DC
DC
DC
DC
DC
DC
DC
NL
SN
SN
SN
SN
SN
SN
SN
SN
SN
SN
SN
WH
WH
WH
2
NL
0:
00
24:45
24:
24:
25:
25:
25:
25:
25:
26:
26:
26:
26:
26:
26:
26:
26:
51
55
16
31
36
42
48
00
10
16
30
34
40
45
49
RO
RO
RO
RO
RO
RO
RO
RO
RO
RO
RO
RO
RO
RO
0.
0.
0.
0.
1.
0.
0.
1.
1.
0.
1.
0.
1.
0.
1.
2.
0.
61
95
69
17
38
90
31
33
00
71
35
18
65
62
50
45
67
Peaks
0:
00
25:30
1.
RO
RO
26:05
26:11
DC
4
NL
26:
:29
1.
4.
0.
0.
70.
6.
0.
0.
0.
0.
2.
0.
2.
0.
2.
16
70
33
29
22 40.70
50 3.60
20
84
76
65
61
13
15
67
55
0.49
0.58
0.939-1.017
0.
0.
0.
0.
29.52 0.
3.98 0.
0.
0.
0.
0.
0.
1.
1.
1.
1.
1.
1.
000
945
949
952
965
975
978
982
985
993
999 123478-HxCDD
003
012 123789-HxCDD
015
018
022
024
AN
AN
76.72
05-1.43
0.
,68
1.50
1.24
1.
1.
Peaks
0
:00
28:18
DC
DC
DC
DC
DC
DC
DC
DC
DC
DC
DC
SN
SN
SN
SN
SN
SN
SN
SN
WH
WH
1
NL
2
28:33
28
28
28
28
29
29
29
29
29
:38
:46
:55
:58
:12
:27
:32
:45
:57
0.
.24
.24
Ajjuve: ;
88-1.20
0.89
RO
RO
RO
RO
RO
RO
RO
RO
1.34
3
1
0
0
1
0
0
0
3
0
.61
.74
.94
.64
.25
.77
.90
.65
.41
.92
Peak
0
28
29
0
:00 RO
:lfi
:34
1.17
8.26 5.53
2,311.33 1,277.38
4,674.07 2,586.91
2,879
.60 1,595.64
0.962-1.038
0.000
3.69 0.974
1,033.95 0.
2,087.16 1,
1,283.96 1
.996 13C12-HXCDD 478
.000 13C12-HXCDD 678
.011 13C12-HXCDD 789
SUR4
IS5
RS2
9,873.26
1
16
0
0
1
0
0
0
0
1
0
1
16
.06
.38 10.80
.77
.55
.03
.35
.33
.39
.57
.02
.35
.40
.38
.37-0.51
1
0
0
.04
.43
.44
Peaks
2
3,881
1,627
5,508
.32
.82 1,173.68
.08 494.64
.90
0.995-1.051
0
8.03 1
1
1
1
1
1
1
1
1
1
1
.000
.000 1234678-HpCDF
.009
.012
.016
.022
.024
.032
.041
.044 1234789-HpCDF
.051
.058
AN
AN
0.929-1.141
0
2,708.14 1
1,132.44 1
.000
.000 13C12-HpCDF 678
.045 13C12-HpCDF 789
IS6
SUR5
Triangle Laboratories, Inc.® Analytical Services Division
801 Cap'rtola Drive • Durham, North Carolina 27713
Phone: (919) 544-5729 • Fax: (919) 544-5491
Printed: 15:53 11/11/96
O 9 r
i-~ ~,«-»
-------
Page No.
11/11/96
Listing of T96660SB.dbf
Matched GC Peaks / Ratio / Ret. Time
Compound/
M_Z.... QC.Log Omit Why ..RT. OK Ratio Total.Area... Area.Peak.1.. Area,Peak.2.. Rel.RT Compound.Name.„ ID.
Above; HpCBF / HpCDD Follows
HpCDD
424-426
424-426
13C12-HpCDD
436-438
436-438
DC
DC
DC
DC
DC
DC
DC
DC
DC
NL
SN
SN
SN
SN
SN
WH
WH
WH
2
0
28
28
28
29
29
29
29
29
29
29
:00
:28
;38
:45
:01
:07
:14
:22
;27
:34
:38
0.
RO
RO
RO
RO
RO
RO
RO
RO
.88-1.20
17
2
0
0
0
1
0
0
1
1
0
.00
.29
.96
.75
.67
.46
.95
.76
.03
.67
.58
Peaks
0
' 1
10
0
1
0
11
0
0
1
0
21
.08
.00
.74
.47
.12
.71
.08
.25
.71
.83
.88
.82
0.88-1.20
DC NL 0:00 1.11 3.02
28:36 RO 0.50 5.08
29:14 1.03 3,636.88
2 Peaks 3,641.96
5.26
5.41
2.60
1,848.98
0.973
5.48
5.67
0
0
0
0
0
0
1
1
1
1
1
-1.006
.000
.974
.979
.983
.993
.996
.000 1234678-HpCDD
.005
.007
.011
.014
0.966-1.034
0.000
5.17 0.978
1,787.90 1.000 13C12-HpCDD 678 1ST
Above: HpCDD / Octa-CDD and CDF Follows
OCDF
442-444
AN
442-444
0.76-1.02
DC NL 0:00 RO 0.45
31:47 RO 1.10
1 Peak
1.21
7.11
7.11
4.13
0.874-1.126
0.000
3.76 1.002 OCDF
OCDD
458-460
458-460
0.76-1.02
DC NL 0:00 1.00 0.06
DC SN 31:34 RO 0.38 0.23
31:43 RO 0.56 24.51
DC SN 32:11 RO 11.11 0.17
1 Peak 24.51
11.53
0.874-1.126
0.000
0.995
20.62 1.000 OCDD
1.015
13C12-OCDD 0.76-1.02
470-472 DC NL 0:00 1.00 0.04
31:43 0.84 4,075.73
470-472 1 Peak 4,075.73
1,864.16
0.995-1.006
0.000
2,211.57 1.000 13C12-OCDD
isa
Column Description "Why" Code Description QC Log Desc.
M_Z -Nominal Ion Mass(es)
..RT. -Retention Time (mratss)
Rat.l -Ratio of M/M+2 Ions
OK -RO=Ratio Outside Limits
Rel.RT-Relative Retention Time
*** End of Report
WL-Below Retention Time Window
WH-Above Retention Time Window
SN-Below Signal to Noise Level
-------
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File:T966S05 #1-835 Acq:l-NOV-96 00:58:37 EI+ Voltage SIR 70T Noiae:1142
317.9389 Fi2 BSUB(256
,30, -3.0J PKD(5,
3,l,0.10%,4568.0,0.001>rF,F) ExpsEPCUS
TRIANGLE LABS Text.-23.B-2 TLI#39291R1 IWJ. TIME - 01 » 02
1001
so:
60:
40:
20:
o-
13 'sOO
14. -00
A4.95E7 _1.2E7
)
i
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';9 . 6E6
"-.7.2E6
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' 15:00 Ifil-Ofl' 17:00 18:00 Time
File:T966605 #1-835 Aeq:l-NOV-96 00:58:37 Eli- Voltage SIR 70T
330.9792 F:2 Exp:EPCUS
TRIANGLE LABS Text:23B-2 TLI#39291R1 JKT. TIME = 01:02
1003
80.
60.
40.
20.
0
•^ 13:15 1 1. 14
j 1 1 1 F- T
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13; 58 14:25
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File:T966605 #1-835 Acq:l-NOV-96 00:58:37 EI+ Voltage SIS 70T
375.8364 F:2 Elp:EPCUS
TRIANSLE LABS Text : 23B-2 TLH39291R1 JKT. TIME <* 01:02
1004
80|
SOJ 1
40J1 1 13:40
-.I 1 13:15 ft
"jijtiji i jlj
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13! 00
14
14 • 02
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17:16
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15-13 |||1 [ lIlAl i7:33\,[ i
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15s 00 ' ' ' 16s 00* 17s 00 ' ' 18-00 Time
00 Q
/-„__/
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F±leiT966605 #1-835 Acgt 1 -SOV-96 00:58:37 KH- Voltage SIX 70T Xoiaes 796
31S.8965 Fs2 BS0S(256t30,-3.Q} PKS(5, 3,1, 0. 101,3184. 0,0.00*,F,F) ExpiEPCOS
TRIANGLE LASS Text:23S-2 TLI#39291X1 IKJ. TIME » Ols 02
1003k
801
sol
401
201
ol
M.
14 f
>3E5
\ A3.31E5
I
2.0E5
\ l\ A1.37E5
\ { A A2.S9S4 A7.35E4
00 ' 15:00 16:00
17:00 18:00
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-4.1S4
.O.OSO
Time
F±le:T96S605 #1-835 Acqtl-NOV-96 00:58:37 EI+ Voltage SIS 70T Noise: 44S
321.8936 F-.2 SSVS(256,30, -3, 0) PKD(5, J,l,0.10%,1792.0,0.00», F,T) SxpsEPCUS
TRIANSLE LASS TeXt:23S-2 TLIt39291Sl JMJ. SIMS •> Oil 02
1004
801
60:
40:
20":
ol
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00 15sOO 15:00
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Time
.File. -TS 66605 #1-835 Acq:l-KOV-96 00:58:37 EI+ Voltage SIS 70T Noiae:3056
331.S368 F-.2 SSUS(256, 30, -3.0) PKD( 5, 3,1, 0 . 101,12224 . 0, 0. 00%, F,F) ExpsEPCUS
TSIAXSLE L&BS Text.:23S-2 TLH39291X1 INJ". TIME = 01:02
100*
sol
601
401
20:
o-
14
A3..
A1.96E7
I
00 15:00 ' ' 16,- 00
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FilesT966605 #1-835 Acqsl-HOV-96 00:58:37 SI+ Voltage SIS 70T Noise: 1220
333.9338 F:2 BSUB(256, 30, -3.0) PKD(5, 3, 1,0. 10%,4880. 0,0.00%, F,F) ExpiEPCDS
TSIAS&LE LABS Text: 239-2 TLIt392SlSl XKJ. TIME « 01:02
1009
80:
6Q:
40-
201
o-
14
A4 . OSS?
A2.48E7
1
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\ .
17:00 18:01
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FilesT9666Q5 #1-835 Acqsl-SQV-96 00:58:37 SI+ Voltagre SIS 70T Noiae:339
327.8847 F:2 BSUB(256, 30, -3. 0) PKD(5, 3,1, 0 ,10\,1356. 0,0. 00*,f ,F) ExpiEPCUS
TRIANGLE LABS Text:23B-2 TLI#39291S1 JMJ. TIME - 01:02
1003
80,
60.
40.
20.
0
A3.
I
1
14\00 ISsOO ' ISsOO
rilesT9SS605 #1-835 Acqsl-HOV-SS 00i58i37 EI+ Voltagre SIM
330.9792 F:2 Xxp:E?CUS
TRIANGLE LABS Text s 2 3 S-2 TLIt39291Rl
1001
80.
60.
40.
20.
0
yj-i
14
^^-^^Lifj^^^^^^ 15,55 16:12
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n f
ft
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IHJ. TIME - Ols 02
££i££iSi£8 17-21 17:57
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'ilesT966605 #1-835 Acq:l-KOV-96 00:56:37 EI+ Voltage SIR JOT Noise: 198
339,8597 F:2 BSUB(256,30r -3. 0) PJOJfS,3,1, 0.10%, 792. 0, 0. 00%,F,F; EipsSPCUS
TRIANGLE LABS Teit:23B-2 TLH39291R1 HKT. TIMS - 01:02
18:00 19:00 20:00 21:00 22:00 23:00
File:T96S605 §1-835 Acq:l-NOV-96 00:58:37 EH- Voltage SIX JOT Noiae:839
341.85S7 F:2 SSVS(256,30, -3. 0} PKD(5,3,1, 0.10%,3356. 0,0. 00%,f",FJ Exp:EPCUS
TRIANGLE LABS Text:23B-2 TLI#39291R1 XKT. TIME = Ols 02
1003. A1.61E5
1S.-00 19:00 20:00 21:00 22:00
File.'2566605 #1-835 Acq:l-NOV-96 00:58:37 EI+ Voltage SIR 7QT Noise:26
351.9000 F:2 BSUB(256, 30, -3 . 0) PKD(5, 3,1, 0.10%,104 . 0, 0. C0%,F,F; ExpsEPCDS
TRIANGLE LABS Text:23B-2 TLI#39291S1 HKT. TIME = 01:02
IOCS A4.86E7
23: 00
802
602
A2.44E7
18:00 19:00 20:00 21:00 22:00
File:T966605 #1-835 Acq: 1 -KOV-96 00:58:37 EH- Voltage SIR 70T Noise:520
353.8970 F:2 BSTJS(256,30,-3,0) PKD(5,3fl, 0.10%,2080. 0,0. 00%, F, F) ExpiEPCUS
TRIANGLE LASS Text: 235-2 3IJ#35291Jil JKT. TIME = 01:02
1003, A3.12E7
23 : 00
802
602
402
202
Al.S5E7
I V
18:00 19:00 20:00 21:00 22:00
File.-TSeSSOS #1-835 Aajil-KOV-96 00:58:37 EI+ Voltage SIR 70T
330.9792 F:2 Exp:EPCUS
TSI&NSLE LABS TeXt:23B-2 TLI#39291X1 JJK7, TIME = 01:02
l?-il20:07 ^££ij£.2ii"21:30 22:06
602
402
202
18:00 ISiOC 20.-00 21:00
F±le:T966605 #1-835 Acqsl-NOV-96 00:58:37 EI+ Voltage SIR 70T
409.7974 F:2 ExpiEPCOS
22:00
23:00
TRIANGLE LABS
100S
Texts23B-2 TLIX39291R1
IKT. TJME -
01«02
23:00
22:32 22:54 23,-16
.OEO
Tine
J.2E4
2.6E4
1. 9E4
1. 3E4
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.O.OEO
Time
.1.1E7
.9.0E6
.6.8E6
.4.5E6
.2.3E6
.O.OEO
Time
.7.3E6
.5.8E6
.4.4E6
.2.9E6
.1. 5E6
.O.OEO
Time
.2.1E7
.1. 7E7
.1. 3E7
.8.4ES
.4.2ES
.O.OEO
18.-00
1S.-00
20:00
21:00
22:00
23:00
30
-------
FilesTSSSSOS tl-835 Aoq-.l-toOv-SS 00:58:37 E~FF Voltage 'W 7St NoiBe:44B
355.8546 F:2 BSOS(2S6r30, -3.0) PXZ
If 5, 3, 1,0. 10%, 1792.0, 0.00%, F,F) ExpsEPCUS
ZRJAHGEE LABS Text:23B-2 TLX939291&1 XJKT. TIME - 01 ."02
1004
•
so:
601
'.
401
201
Q
A2.52E5
-4.4E4
A A2.Q7E5
\
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' 20; 00 ' ' 21s 00 ' ' ' ' 32s 00 ' 23:00 Tiae
File:T96660S #1-835 Acqsl-NOV-96 00:58:37 EI+ Voltage SIS 701 Noiaesl70
357.8515 ti2 SSU3(25Se30, -3.0) PXD(5, 3, 1,0 ,101,680. 0,0. 00%fW,W) ExpsEPCUS
TRIANGLE LASS Text: 238-2 TLI #39291X1 IJET. TIME ' 01:02
1003, A1,9SE5
801
601
401
201
0'
/
4.1S4
A1.22E5
t
1
I [ A1.82E4 1
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rJ \. .,^U- ^^N^A^.V
A7.23E4
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fl.OEO
20:00 ' 21s 00 ' 22\-00 23 1-00 ' ' Time
File:T966605 #1-835 Acqil-NOV-96 00:5Bs37 EI+ Voltage SIR 7 OT Noises 24 5
367,8949 F:2 BSUB(256,30,-3.0) PKX>(5, 3,1, 0.10*, 980. 0, 0.00*,F,F} Exp:EPCUS
TRIANGLE LABS Text:23B-2 TLH39291R1 IWJ. TIME - 01 .- 02
1004
ao:
so:
401
201
01
A2.59E7
|
M
A2.40Z5
/ \/v
S.7E6
15.4£6
L4.0S6
'.2.7E6
'.1.3E6
' 0 . OEO
20.-00 21:00 22sOO ' ' ' 23sOO ' ' Time
File:T966605 #1-835 Acq:l-NOV-96 00:58:37 EI+ Voltage SIR 70T Noiae:21
369,3919 T:2 BSUB(256r30, -3.0) PXD(5, 3,1,0 ,10\, 84.0,0.00%,F,F; Exp:EPCUS
TRIANGLE LASS Texts23B-2 TLI#39291X1 TOT. TIME » Oil 02
1003
801
601
401
20.
0.
Jil . 74JET7
A
L ™
/ \yV*
4.5E6
,3 . 6E6
-2.7E6
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-9.0E5
' O.OKO
20:00 21s 00 22»00 23«00 Tiae
Jtile.-T9S6605 #1-835 Acq:l-HOV-9S
330.9792 Fs2 Exp:SPCUS
OOi58lJ7 n* vojtdgre SIS 70r
TBIAUGZE LABS Tmxts239-2 TZH39291X1 OTJ. TIME - 01:02
1003
80.
SO.
40.
20.
0.
20:03 20:4,
20:00
'—- ^i^i-iii" ,-Z^y^~-^mi~^i3°!>i "'"
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-1.2E7
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O.OEO
21:00 22»00 23:00 Time
231
-------
File8!T566605 #1-505 Acq:l-NOV-96 00:58:37 EI+ Voltage SIS 70T No±ae:594
373.8208 F:3 BSUB(256,3Q,-3.0) PKD(5, 3,1, 0.10%,2376. 0, 0 . 00%,F,F) ExpsEPCUS
TXIANSLB LABS Text:23B-2 TLH39291S1 IJKT. TIME= Ols 02
1003
80J
24:00 25:00 26:00 27:00
F±lesT966605 #1-505 Acq:l-NOV-96 00:58:37 EI+ Voltage SIS 70T Koiae:639
375.8178 F:3 BSUB(256,30,-3.0) PKD(5,3,1,0.101,2556.0,0.00*,F,F) Exp:EPCUS
TRIASSLE LABS Text:23B-2 TLH39291K1 I1TJ". TIME - 01:02
1003* A6.11E4
A4-I9E4 A4.20E4
24': 00 25:00 26:00
File:T966605 #1-505 Acqil-XOV-96 00:58:37 EI+ Voltage SIS 70T Noise:508
383.8639 Fs3 SSOB(256,30, -3.0} PXD(5,3,1, 0.10%,2032,0,0,00%,F,F) Exp:E?CDS
TRIANGLE LABS Text:23B-2 TLI#39291S1 IKT. TIME = 01:02
1004
O.OEO
Time
27:00
aft:
40
201
A9.B3ES
A8.23E6
24:00 25,-00 ' 26s00 '
File:T966605 #1-505 Acq:l~NOV-96 00:58:37 EI+ Voltage SIR 70T Noise:521
385.8610 F:3 BSUB(2S6, 30, -3. 0} PKD($,3,1,0.10%,20B4 .0,0. 00%,F,F) Exp:E?CUS
TRIASSLE LABS Texts233-2 TLI#39291R1 HKT. TIME " 01:02
100^ A3.69E7
27s 00
40:
20:
ol
A2.04E7
Al. 70E7
24:00 25:00 26:00
File:T966605 #1-505 Acq:l-SOV-96 00:58:37 EI+ Voltage SIS 70T
392.9760 F:3 Exp:EPCUS
TRIASSLE LABS Text:23B-2 TLI#39291S1 HOT. TIME = 01:02
24:52 25:09 25:31 25:45 25:01 26il4 26:31 26:45
r- '"VV»'-VV'^V^'"~W^^v-^v~-''V^'N/**A^v'V"v~^^ J~
80j
60:
40.
20:
0:
27:00
27: 02
.5.4E6
.4.3E6
.3.2E6
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.1.1X6
.O.OEO
Time
.1.1X7
.8.8E6
.6.6E6
.4.4E6
.2.2E6
.O.OEQ
Time
.1. OE7
.S.2E6
.6.2E6
.4.1E6
.2.1E6
.0.0X0
24:00 25:00 26:00
FiltnT966605 #1-505 Acqsl-SOV-96 00s58i37 EI+ Voltage SIS 70T
445.7555 F:3 ExpiEPCUS
TRIANGLE LABS Text:23B-2 TLI#39291R1 UKT. TIME
1003*
24:57
27:00
01:02
24:00
25:00
26:00
27s 00
-------
T966605 #1-505 Acgsl-SOV-96 00:58:37 EI+ Voltage SIS 70T
392.9760 F:3 Exp:EPCUS
2612 2624 2636 2S.-48
25:31
25.-4S
TRIANGLE LABS
100*
so:
60:
40:
20:
Tezt:2JB-2 HI #39251X1
ISJ. TIKE = 01:02
26:01 26.-14 26:31 26:45
rr
rr
rr
.1.2X5
.9. 8X4
.7.3E4
.4.9.E4
.2.4X4
.O.OEO
Time
.9. 6S4
.7.7E4
.5.7E4
.3. 8E4
.1. 9E4
.O.OEO
Time
16.6E6
.3.3ES
.1. 6E6
O.OEO
Time
24:36 24.-4S 25sOO 25»12 25:24 25:36 25:48 26:00 26.-12 26:24 26:36 26.-4S
.6.6ES
.5. 3E6
.4.0E6
.2.6E6
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Time
.1. OE7
.8.1E6
.6.1X6
.4. 1X6
.2.0£6
.O.OKJ
Tine
233
-------
*ile:T966605 #1-443 Acqsl-NQV-96 00:58:37 EI+ Voltage SIS 70T Koiees250
407.7818 F:4 BSUB(256,30, -3.0} PJOJf5,3,l, 0.10%,1000. 0,0,00%,F,F.) ExpsEPCUS'
TRIANGLE LABS Textt23B-2 TLI#39291S1 JPCT. TIME - 01:02
100J
80:
60:
28:12 28:24 28:36 28:48 29:00 29:12 29:24 29:36
FilesT966605 #1-443 Acq-.l-NOV-96 00:58:37 EH- Voltage SIX 70T lfoi.se.-279
409.7789 Tst BStJB(256,30,-3.0) PKD(5,3,1,0.10%,1116.0,0.00%,,F,.F) EjcpiEPCUS
TRIANGLE LABS Text.-23.B-2 TLI#39291S1 JJW7. TIKE = 015 02
1004
28:12 28:24 28:36 28:48 29:00 29:12 29:24 29:36
File:T9S660S #1-443 Acq:l-NOV-96 00:58:37 EH- Voltage SIM 70T Soise:838
417.8253 F:4 BSUB(2S6,30,-3.0) PKD(5,3,1, 0.10%, 3352. 0, 0. 00*,F,r) Exp:EPCUS
TRIANGLE LABS Text.-23.B-2 TLH39291K1 IKT. TIME • 01:02
1004 A1.J.7E7
40:
20:
o-
A1.10E5
_J.1£5
-8.4E4
•.6.3E4
-4.2E4
-2.1E4
A6.74E3
25:48
30.-00
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A2.60E3 A4.95E3 A8.01E3 A1.66E3
29:48
60:
40:
20:
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A4.95E6
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"-8.8E3
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30:00 Time
4.1E6
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-8.1E5
28:12 28:24 28:36 28:48 2S.-00 29:12 29:24 29:36
F±le:T96660S #1-443 Acg: 1 -HOV-96 00:58:37 EI+ Voltage SIS 70T lfoise:803
419.8220 F:4 BSOB(256,30,-3.0) PKD(5,3,l,0.10*,3212.0,O.OOlrr,r) Exp:EPCOS
TRIANGLE LABS Text.-23.0-2 TLI#39291R1 IHT. TIME - 01:02
1004 A2.J1S7
80:
29:48
30:00
-O.OEO
Time
60:
40.
20:
0~
Al. 13E7
^3.2E6
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.5. 5E6
13. 7ES
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28:12 28:24 28:36 2B.-48 29:00 29il2 29I-24
F±le:T966605 #1-443 Acg:l-KOV-96 00:58:37 EI+ Voltage SIR 70T
430.9729 F:4 Exp-.EPCUS
TRIANGLE LABS Teit:23B-2 TLI#39291R1 INJ". TIME
29:36
29:48
BO:
so:
40:
20:
o:
01:02
9:39 29'50
30:00
30:00
O.OEO
Time
-6.8E6
-.5.5E6
-4.1E6
'-.2.7E6
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28sl2 28:24 28:36 28:48 29:00 29:12 29:24
FilesTSS6605 #1-443 Aoq:l-SOV-96 00:58:37 EH- Voltage SIS 70T
479.7165 f:4 Eip:OPCUS
TRIANGLE LABS Text:23B-2 TLI#39291R1 JWJ". TIME
29:36
01102
29:48
30:00
-O.OEO
Time
1004
28; 50
28:12
28:24
28:36
28:48
29:00
29112
29:24
29:36
29:48
30:00
34
-------
28.-30 28:35 28:42 28-48 28-S4 29:00 29:06 29.-12 2SJ18 29:24 29:30
File:TSS6605 #1-443 Acqtl-SOV-96 00:58:37 EI+ Voltage SIS 70T Woi»es20
425.7737 F:4 BSUB(256,30f -3.0) PJCDf5,3,l, 0.10%, 80.0, 0. 00\,F,F) ExpsEPCBS
TRIANGLE LABS Teit:23B-2 TLI#39291X1 INJ. TIME - 01:02
100J
so:
"il-443 Acq:l-ltov-§6 60:5B:37 Si* Voltage "sJs 70S Jteiae:J4l
23.7766 T:4 BSVS(256,30,-3.0) PKD{5,3,1,0.101,1364.0,Q.OO\,f,r) ExpsEPCOS
TRIANGLE LABS Teit:23B-2 TLIf39291X1 JKT. TIME = 01:02
004 A5.41E4
2S:36 2942
0.
85E7
28:30 28:36 28:42 28:48 28:54 29:00 29:06 29.-12 29:18 29:24 29:30 29:36
File:T966605 #1-443 Acqsl-NOV-96 00:58:37 EI+ Voltage SIR 70T No±ae:794
435.8169 F:4 BSUS(256,30,-3.0) PXB(5,3,1,0.10%,3176.0,0.00%,F,F) Exp-.EPCUS
TRIANGLE LABS Text: 23B-2 raJ#39291JTl XIKT. TIME = 01:02
JOO* AH
801
601
40.
201
29:4.2
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Time
r-6.
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^3.
3E6
1E6
8E6
-2.5E6
'.1.3E6
.O.OEO
28:30 28':36 28s42 28:48 2S.-54 291-00 29:06 29:12 29:18 29:24 29i30 29:3S 291-42 Time
FileiT966605 #1-443 Acq:l-NOV-96 00:58:37 EI+ Voltage SIS 7QT Noise: 715
437.8140 F:4 BSUB(256,30,-3.0) FJO3f5,3,l,0.10%,2850. 0, 0, QQ*,FrF) Exp-.EPCUS
TRIANGLE LABS Teit:23B-2 TLI#39291S1 JJW. TIME " 01:02
100* A1.79E7
801
601
401
20.
0.
-6.1E6
-4.9E6
'.3. 6E6
'.2.4E6
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28:30 28:36 28:42 28:48 28:54 29:00 29:06 29:12 29:18 29:24 29J30 29.-3S 29:42
File:T966605 #1-443 Acq:l-SOV-96 00:58:37 EI+ Voltage SIS 70T
430,9729 F:4 Exp:EPCUS
TRIANGLE LABS Texts23B-2 TLH139291X1 IHJ. TIME - 01:02
Time
1001
BO:
601
40.
20.
28:34
^6.8E6
.5.4E6
'.4.1X6
.2.7m
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28:30 28:36 2S.-42 28:48 28:54 29:00 29:06 29sl2 29:18 29:24 29:30 29:36 29:42
O.OEO
Time
-------
File:T966605 #1-443 Acqil-NOV-96 00:58:37 EH- Voltage SIR 70T Jfoiae:2S3
441.7428 F.-4 SSUS(256,30,-3.0) PKD( 7,2, 3, 0.10%, 1132. QrO.QO*,r,F) SxpsEtCOS
TRIANGLE LABS Texts23B-2 TLH39291S1 IMT. TIME - 01 .-02
IOCS
29:00 JOsOO 31:00 ] 32:00
T±le:T96S605 #1-443 Acq:l-SOV-96 00:58:37 EI+ Voltage SIB 70T Noise:636
443.7399 F:4 BSUB(256,30, -3. 0) PKD(7,2,3,0 .101,2544. 0, 0. 00%,F,f; Exp:EPCUS
TRIANGLE LASS Texti23B-2 TLX#39291R1 XWJ. flftE = Oil02
1004 !
33s 00
29:00 30:00 31:00
FilesT9S6S05 #1-443 Acg:l-KOV-9S 00:56:37 EI+ Voltage SIS 70T \
430.9729 F:4 XxptSPCUB \
TRIANGLE LABS Text:23B-2 TLXH39291S1 XWJ. TIME
1004 Ta.^e 29:09 30:1230:30
32s 00
33 s 00
901
80J
701
601
501
401
301
201
101
01
28.-45
30:56
31:36
01:02
32:0032:19
33s 10
29:00 30:00 31:00 32:00
Tile:T966605 #1-443 Acgil-HOV-96 00.-58.-J7 EI+ Voltage SIR JOT
513.6775 F:4 ExpiEPCUS
TSIANGLS LABS Text:23B-2 TLX#39291S1 ITKT. TIME =
30 10
33s 00
6.
9E6
2E6
SES
BE6
2ES
SES
8ES
1SS
4E6
9E5
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Time
29:00
30:00
31s 00
32s 00
23G
-------
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57.7377 r-.4 BSUB(256, 30, -3.0) PKD(7,2,3,0.10\,60.0,0.00\,T,T) EzptEPCUS
TRIANGLE LABS Teit:23B-2 TLI#39291R1 INJ. TIME =
004 A1.15E5
BO:
601
401
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31:36 31:42 31:48 31:54 32:00
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459.7348 F:4 BSUBf 256,30, -3.0) PKD(7,2,3, 0.10%,56. 0, 0. 00*,F,T) Ezp:SPCVS
TRIANGLE LABS Teit:23B-2 TLI#3929lRl INJ. TIME =
1004 A2.Q6E5
801
601
401
201
01:02
20:
A8. 72E3
A4.85E3
32:06
01: 02
~r
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31:36 31:42 31:48 31:54 32:00
File:T966605 #1-443 Acq:l-NOV-96 00:58:37 EI+ Voltage SIR 70T Noise: 10
469.7779 F:4 BSUB(256, 30,-3 .0 ) PKD( 7,2, 3, 0 .10%, 40. 0, 0. 001,F,F) Elp:EPCUS
TRIANGLE LABS Teit:23B-2 TLH39291S1 INJ. TIME =
J004 A1.86E7
80.
60.
40.
20.
32:06
01: 02
31:36 31:42 31:48 31:54 32:00
Tile:T966605 #1-443 Acq:l-NOV-96 00:58:37 EI+ Voltage SIR 70T Noise:12
471.7750 F:4 BSUB(256, 30, -3 . 0) PKD(7,2,3, 0.101,48 .0, 0.00*,F,F) Exp:EPCVS
TRIANGLE LABS Text:23B-2 TLI#39291R1 INJ. TIME =
1001. A2.21E7
801
eo:
32:06
01: 02
40L
20:
32:08
31:36 31:42 31:48 31:54 32:00
File:T966605 #1-443 Acq:l-NOV-96 00:58:37 EI+ Voltage SIS 70T
430.9729 F:4 Exp-.EPCUS
TRIANGLE LABS Text:23B-2 TLI#39291S1 INJ. TIME
100* _x^A^f^__^^ 31:52 31:55 32:00
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401
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Text : 23B-2 m|3 9 2 9 1R1 INJ. TIME = 01:02 File Text:23B-2
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15:24
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Time
30!
.8987 F:2 BSUB{256,30,-3 . 0} PKD{7,3,1, 0,10%,5168.0,0.00%,F,T) Exp:EPCUS
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14:12 14:24 14:36 14:48 15:00 15:12
File:T966605 #1-835 Acq:l-NOV-96 00:58:37 EI-i- Voltage SIR 70T
315.9419 F:2 Exp:EPCUS
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311.9389 F:2 Exp:EPCUS
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File:T966605 f1-835 Acq:l-NOV-96 00:58:37 EI+ Voltage SIR 70T
319.8965 F:2 Exp:EPCUS
Sample Text:23B-2 TLIt3929lRl ., -==^ INJ. TIME =
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15:42 15:48 15:54 16:00 16:06 16:12 16:18 16:24 16:30 16:36 16:42 16:48 16:54 Time
File:T966605 #1-835 Acq:l-NOV-96 00:58:37 EI+ Voltage SIR 70T
321.8936 F:2 Exp:EPCUS
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331.9368 F:2 Exp:EPCUS
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F%le:T966605 #1-835 Acq:l-NOV-96 00:58:37 EI+ Voltage SIR 70T
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373.8208 F:3 Exp:EPCUS
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383.8639 F:3 Exp:EPCUS
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-------
TLI Project:
Client Sample:
39291rl
23B-2
Method 23 TCDD/TCDF Analysis (DB-225)
Analysis File: X964237
Client Project:
Sample Matrix;
TLI ID:
Eastern Ridge Lime Facility
M23TRAIN Date Received: 10/19/96
143-23-5A,B Date Extracted: 10/21/96
Date Analyzed: 11/01/96
Spike File: SPC2NF08
ICal: XF21266
ConCal: X964226
Sample Size:
Dry Weight;
GC Column:
1.000
n/a
DB-225
Dilution Factor: n/a
Blank File: T966616
Analyst: JF
% Moisture: n/a
% Lipid: n/a
% Solids: n/a
2,3,7,8-TCDF
0.02
0.85
20:22
13C,2-2,3,7,8-TCDF
6.6
82.3
40%-130%
0.79
20:20
»e,2-l,2,3,4-TCDD
0.80
19:23
Data Reviewer
Page 1 of 1
11/11/96
C2NF.PSR vt.M. LARS 6.08.00
Triangle Laboratories, Inc.®
801 Capitola Drive • Durham, North Carolina 27713
Phone: (919) 544-5729 • Fax: (919) 544-5491
Printed: 16:13 11/11/96
251
-------
Initial
Date..
Data Review By:
calculated Noise Area;
7.00
The Total Area for each peak with an ion abundance ratio outside
ratio limits has been recalculated according to method requirements.
Page No.
11/01/96
Listing of"X964237B.dbf
Matched GC Peaks / Ratio / Ret. Time
Compound/
M_Z.... QC.Log Omit Why ..RT. OK Ratio Total.Area... Area.Peak.1.. Area.Peak.2.. Rel.RT Compound.Name.. ID.
TCDF
304-306
304-306
13C12-TCDF
316-318
316-318
13C12-TCDD
332-334
DC NL 0
16
DC SN 16
17
17
17
17
DC SN 17
17
17
18
18
18
18
19
19
19
DC SN 19
19
DC SN 20
20
20
20
20
0,
:00
:11
:50 RO
:06 RO
:14 RO
:20 RO
:30 RO
:38 RO
:47 RO
:55 RO
:00
:11 RO
:20 RO
:42
:04
:20 RO
:32
:44 RO
:52 RO
:00 RO
:22
:31
:44 RO
:S1
.65-0.89
0.65
0.80
1
1
0
0
0
0
1
0
0
0
0
0
0
0
0
1
0
2
0
0
0
0
19 Peaks
DC NL 0
DC WL 19
19
20
20
DC SN 20
20
DC WH 21
DC WH 22
0
:00 RO
:06
:20 RO
:20
:31 RO
:41 .RO
:52
:23
:08
.06
.41
,62
'.58
.57
.40
.12
.60
.72
.62
.95
.71
.76
.96
.69
.33
.46
.01
.85
.84
.64
.76
1
11.75
98.47
4.58
66.97
63.41
113.61
50.29
4.64
63.21
103.78
32.62
159.12
55.80
227.99
88.61
78.76
67.89
8.17
54.70
3.29
58.38
72.24
36.66
67.53
,560.04
43
53
27
49
21
39
44
13
68
29
94
38
42
27
23
26
32
15
29
.66
.31
.61
.26
.80
.95
.92
.68
.98
.95
.88
.13
.71
.83
.84
.83
.89
.94
.10
54
37
44
85
38
35
75
18
111
31
133
50
44
40
51
31
39
24
38
.65-0.89
4
0
0
0
0
0
0
0
0
4 Peaks
DC NL 0
18
0
:00 RO
:07 RO
.01
.80
.94
.79 22
.55
.98
.81
.75
.74
22
.65-0.89
4
1
.48
.00
2.00
67.83
ISO. 59
,551.36
62.95
14.98
228.87
17.89
335.94
,993.77
TCJDF /
1.81
61.07
80
9,929
27
102
.19
.06
.45
.39
84
12,622
49
126
0.
.81
,88'
.47
.38
.46
.76
.47
.94
.89
.53
.11
.48
.50
.06
.69
.55
.35
,93
.43
0.
.86
.30
.72
.48
788-1.094
0.000
0.796
0.
0.
0.
0.
0.
0.
0.
0.
0.
0.
0.
0.
0.
0.
0.
0.
0.
0.
1.
1.
1.
1.
828
841
848
852
861
867
875
881
885
894
902
920
938
951
961
970
977
984
002 2378-TCDF AN
009
020
025
951-1.049
0.
0.
0.
1.
1.
1.
1.
1.
1.
000
939
951
000 13C12-2378-TCDF ISO
009
017
026
052
089
34
.55
34
0.
896-1.104
0.
.45 0.
000
944
Triangle Laboratories, Inc.® Analytical Services Division
801 Capitola Drive • Durham, North Carolina 27713
Phone: (919) 544-5729 • Fax: (919) 544-5491
Printed: 21:06 11/01/96
-------
Page No.
11/01/96
Listing of X964237B.dbf
Matched GC Peaks / Ratio / Ret. Time
Compound/
M_Z.... QC.Log canit Why . .RT. OK Ratio Total,Area.,. Area, Peak. 1.. Area.Peak.2,. Rel.RT Compound. Name. . ID,.
6,877.94 8,667.44 1.000 13C12-2378-TCDD IS1
4,375.50 5,502.39 1.010 13C12-1234-TCDD RSI
1.023
81.07 112.49 1.045
1.088
1.132
332-334
19:11
19:23
DC SN 19:37 RO
20:03
DC SN 20:52
DC WH 21:43 RO
4 Peaks
0.79
0.80
0.92
0.72
0.78
0.25
15,545.38
9,877.89
13.97
193.56
18.94
13.50
25,677.90
Column Description "Why" Code Description. QC Log Desc.
M_Z -Nominal Ion Mass(es)
..RT. -Retention Time (mm:ss)
Rat.l -Ratio of M/M+2 Ions
OK -RO=Ratio outside Limits
Rel.RT-Relative Retention Time
End of Report
WXi-Below Retention Time Window
WH-Above Retention Time Window
SN-Below signal to Noise Level
-------
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-------
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801
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401
201
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Film:X964237 91-784 Acgt l-NOV-1996 19:39:20 OC El* Voltage SIR AutoSpec
375.8364 Srp:XCONF_TT
Sanfl» T*Xt:23B-2 TLI«39291rl Film TuxttTRUOKILS LABS
19 ill
22:00
1.8ES
.l.SES
.LIES
7. 3E4
.3. 6S4
O.OEO
Time
.2.1S7
.1.7E7
.1.3E7
.8.SE6
.4.2S6
.O.OEO
Timm
.2.8E7
.2.2E7
.1.727
1.127
',5.5E6
.0. OEO
Time
16:00
17:00
18:00
19:00
20:00
21:00
22:00
235
-------
7Ua":XSe"4237 #1-784" Aoq: l-tttV-1996 19:39:20 OS JET*
319.8965 BSm(25S,3Q,-3.0) HOJf5,3,l, 0.10%, 7948. 0, 0
Voltage SIR Auto^poc Noise: 1387
.QaX,P,F) ExptXCONF_TT
Sample Tmxt:23B-2 TLI#39291rl File Text : TRIANGLE LABS
100*
801
SOI
'•
401
201
,
17
A7.43ES
I
\ [I A1.5SES JU.
&L.78E4 / U . L, Au AS-^4B4 .A
J_&^4^^LJiMrAJw-1_^yrv-sJ\/Vi jj^ A^-n^
•00 IBiOO 19:00
Fila:X964237 #1-784 Acqi l-SOV-1996 19:39:20 OC EI+
321.8936 BSVB(2S6,3Q,-3.0) Ha3f5,3,l,Q.10*,S108,0, 0
8SES
^ML.5BS4 A7'p£* A2.8SE4 A2.48S4 A3.43E4
-3.9ES
-3.1ES
-2.4ES
-1.6ES
-7.9E4
o.oso
20:00 21:00 Time
Voltage SIR AutoSpec Noise:2277
,OOX,P,F} Exp:XCONF_'PT
Saaplo T«xt:23B-2 TLI#39291rl Film Taxt:TRIASOLS LABS
IOCS
so:
SOI
".
401
201
n~
j
17
\
A8*53B5
A
t j 1 A2.9SSS A4~
Ai-f354Lu. ~ J^^5_j*JZj£S.
FilasX964237 #1-784 Acqi l-NOV-1996 19s39:20 OC EH-
01ES
kg, A8.SSE4 A3.04E4 «•"•"
_.1lS^ ^.^^ A^^v^A^^u^^a^AvW^^-A-^^^
-4.3E5
.3 . 4SS
12.6E5
11.7SS
'.8.SE4
" n . onn
T^nm^,r , .ttp,. "-^plB --" J.T, an', , n) „ ', i ., t ...,..— :.—,^, urn. 01 ]^xz=r-, r-— ™— , ,,n..J^sa — - - — -
20.- 00 21 ,-00 Time
Voltage SIR AutoSpec No±se:423
327.8847 BSUB(2S6,30, -3,0) PKD(S,3,1,Q,1Q'*,1692.0IQ,00*,F,F) ExpsXCOHF_7T
Sample
IOCS
801
SOI
401
201
0'
17
Taxt:23B-2 TLI#3S2Slrl File Text -.TRIANGLE IABS
A8.61E7
\
/ I
:00 iai-00 15sOO
-1.7E7
-1.3E7
L9.9ES
16. 6E6
"-3.3E6
" O.OSO
'20iOo' ' . ' '21:00 Time
Fil»:X9S4237 #1-784 Acq: 1-8OV-1996 19:39:20 OC BI+ Voltage SIR AutoSpec Noisa:22B3
331.9368 BSUB1256,30,-3.Q) PKD(5,3,1, 0. 101,9132, 0, C
Sample
ion
801
601
401
20.
0
1. 00%, F, F) EXp:XCONF_TT
T*xt:23B-2 TLI#39291rl File Text : TRIASQLE LABS
A6.88E7
1
1 l '
1
J V
' i7\oo' isioo is.-oo'
38E7
h
'
••
\ _
-1.3E7
11.1B7
".7.9E6
IS.3E6
'.2.6E6
' 0. OTSO
20»0o' ' ' '21*00 ' Tiao
F±lm:X964237 01-784 Aeq: l-SOV-1996 19:39:20 OC JBT* ValCSffm SIS AutoSpec SoismsSlO
333.9338 BSVB(256,30,-3.0) PKD
-------
ile:XS64237 #1-784 Acgi 1-8OV-1396 19s3S:20 OCJET* Voltmffm SIS AutaSpea
03.9016 S*p:.XCOHF_rr
anpla Taxts23B-2 TLX#39291rl Pile TextsTRXANOLS LABS
16:00 17:00 ltt:OO ISsOO 20*00 21sOO
'ile:X964237 #1-784 Acq: l-KOV-1996 19:39:20 OC EI+ Voltage SIR AutoSpoc
15.9419 Exp:ZCOSF_TT
triple Tmxt:23B-2 TLX#39291rl Pile Text:TRIANQLS LABS
100* 20,20
80J
601
40:
20:
22 i 00
16:00 17:00 18:00 19:00 20:00 21:00
'ile:X964237 91-784 Acq: l-NOV-1996 19:39:20 OC JET* VoltaffB SIR AutoSpec
319.8965 Exp:XCONF_TT
Taxt:23B-2 TX,X#3929irl Fil» foxt:TRIASOIiB LABS
22:00
15:00 17s00 18:00 1SJOO 30.-00 21:00
Film:X964237 #1-784 Acqs l-SOW-1996 19s3St20 OC EI+ Voltmga SIR AutoSp»e
331,9368 Exp:XCONF_TT
Saapl* Taxt:23B-2 TLX#39291rl Pile TmxtiTRIANGLE LABS
100*
sol
eol
40:
20!
a- ...
22s 00
16:00 17:00 18:00 15:00 20JOO 21:00
File:X964237 #1-784 Acq: l-KOV-1996 19:39:20 OC Sit- Voltage SIR AutoSpec
292.9825 Exp:XCQNP_¥T
Sample Tmxt:23B~2 TLI#39291rl Pile TextsTRIANQLS IABS
l-e:12j6:3617j01^ ^J:7jl°.l? 112 _ IfliSS 19t41 20:06 _
80:
60:
40:
20:
ol
22:00
~r
—
~r
16:00 17:00 10:00 ISiOO 20:00 21:00
filetX964237 #1-784 Acqs l-HOV-1996 13:39:20 OC ST+ Voltage SIR AutoSpmc
330.9792 SxptXCOSP_TT
S«fflpl» T*3tts23B-2 TLX#3S291rl Film Text:TRIANGLE LABS
'22:00
1003
80:
eol
40:
20l
ol
16
16:3617:00
17:42
18:20
15:48
<00
I7SOO
18:00
15:00
20:00
21:00
-i \ 1 r
22:00
.2.1B7
1.7B7
.1.3B7
3.5E6
4.2E6
O.OEO
Time
.O.OEO
Tim*
.7.9E6
.5.3E6
'.2.6E6
O.OEO
8.5E7
.6.8E7
-5.1ET7
-3.4S7
.1. 7S7
O.OEO
Tim
-7.7E7
:6.UE7
.4.6E7
L3.1S7
'.1.SE7
O.OSQ
Time
-------
Peak Locate Examination: l-NOV-1996:19:38 File:X964237
Experiment:XCONF_TT Function:1 Reference:PFK
Volts
0.7151
292.95315
292.98245
293.01175
330.94615
330.97925
331.01235
-------
TLI Project: 39291rl
Client Sample: 23B-3
Method 23 PCDD/PCDF Analysis (a)
Analysis File: T966612
Client Project:
Sample Matrix:
TLI ID:
Sample Size:
Dry Weight:
GC Column:
Eastern Ridge
M23TRAIN
143-23-6A-C
1.000
n/a
DB-5
Lime Facility
Date Received:
Date Extracted:
Date Analyzed:
Dilution Factor:
Blank File:
Analyst:
10/19/96
10/21/96
11/01/96
n/a
T966616
BD
Spike File:
ICal:
ConCal:
% Moisture:
% Lipid:
% Solids:
SPX23708
TF53286
T966598
n/a
n/a
n/a
2,3,7,8-TCDD
1,2,3,7,8-PeCDD
1,2,3,4,7,8-HxCDD
1,2,3,6,7,8-HxCDD
1,2,3,7,8,9-HxCDD
1,2,3,4,6,7,8-HpCDD
1,2,3,4,6,7,8,9-OCDD
2,3,7,8-TCDF
1,2,3,7,8-PeCDF
2,3,4,7,8-PeCDF
1,2,3,4,7,8-HxCDF
1,2,3,6,7,8-HxCDF
2,3,4,6,7,8-HxCDF
1,2,3,7,8,9-HxCDF
1,2,3,4,6,7,8-HpCDF
1,2,3,4,7,8,9-HpCDF
1,2,3,4,6,7,8,9-OCDF
ND
EMPC
ND
ND
ND
0.04
EMPC
0.14
ND
ND
0.03
0.008
EMPC
ND
0.03
ND
0.06
0.01
0.03
0.02
0.02
0.008
0.34
1.16 29:16
0.89 15:40
0.01
0.01
0.02
0.03
0.01
1.43
1.31
0.95
0.95
25:15
25:23
28:20
31:48
B
Total TCDD
Total PeCDD
Total HxCDD
Total HpCDD
Total TCDF
Total PeCDF
Total HxCDF
Total HpCDF
0.61
0.12
0.13
0.04
1.2
0.26
0.05
0.03
6
2
1
1
10
5
3
1
0.62
0.31
0.15
0.06
1.3
0.28
0.09
Page 1 of2
X237_PSR vl ,14. LARS S.08.00
Triangle Laboratories, Inc.®
801 Capitola Drive • Durham, North Carolina 27713
Phone: (919) 544-5729 • Fax: (919) 544-5491
Printed: 16:05
-------
TLI Project: 39291rl
Client Sample: 23B-3
Method 23 PCDD/PCDF Analysis (a)
Analysis File: T966612
13C12-2,3,7,8-TCDF
13Ci2-2,3,7,8-TCDD
l3e,2-l,2,3,7,8-PeCDF
»Ci2-l,2,3,7,8-PeCDD
13Ci2-l,2,3,6,7,8-HxCDF
13C,rl,2,3,6,7,8-HxCDD
13C,2-l,2,3,4,6,7,8-HpCDF
13C12-l,2,3,4,6,7,8-HpCDD
13C,2-1,2,3,4,6,7,8,9-OCDD
5.2
5.0
4.5
4.5
5.8
5.6
5.4
5.7
8.2
64.6
63.0
56.5
56.6
72.0
70.6
67.0
71.2
51.1
40%-130%
40%-130%
40%-130%
40%-130%
40%-130%
40%-130%
25%-130%
25%-130%
25%-130%
0.75
0.78
1.45
1.49
0.48
1.23
0.40
1.00
0.91
15:37
16:25
20:53
22:20
25:21
26:11
28:19
29:15
31:43
37CL,-2,3,7,8-TCDD
»C,2-2,3,4,7,8-PeCDF
13C,2-l,2,3,4,7,8-HxCDF
13Ci2-l,2,3,4,7,8-HxCDD
13C,2-l,2,3,4,7,8,9-HpCDF
5.3
4.9
5.6
5.0
5.1
133
123
139
124
128
70%-140%
70%-140%
70%-140%
70%-140%
70%-140%
1.41
0.48
1.23
0.40
16:26
21:52
25:15
26:06
29:35
13C,2-l,2,3,7,8,9-HxCDF
13Ci2-2,3,4,6,7,8-HxCDF
4.1
3.8
104
94.4
40%-130%
40%-130%
0.47
0.48
26:42
25:57
13C,2-1,2,3,4-TCDD
l3C,2-l,2,3,7,8,9-HxCDD
0.78
1.26
16:11
26:30
Data Reviewer
11/11/96
Page 2 of2
X237JPSR *I.I4, LARS 6.08.00
Triangle Laboratories, Inc.®
801 CapWola Drive « Durham, North Carolina 27713
Phone: (919) 544-5729 • Fax: (919) 544-5491
Printed: 16:0511/11/96
2HO
-------
TLIProject: 39291rl
Client Sample: 23B-3
Toxicity Equivalents Report
Analysis File: T966612
Client Project:
Sample Matrix:
TLIID:
Sample Size:
Dry Weight:
GC Column:
Eastern Ridge Lime Facility
M23TRAIN Date Received: 10/19/96
143-23-6A-C Date Extracted: 10/21/96
Date Analyzed: 11/01/96
1.000 Dilution Factor: n/a
n/a Blank File: T966616
DB-5 Analyst: BD
Spike File:
ICal:
ConCal:
% Moisture:
% Lipid:
% Solids:
SPX23708
TF53286
T966598
n/a
n/a
n/a
Anafytes
2,3,7,8-TCDD
1,2,3,7,8-PeCDD
1,2,3,4,7,8-HxCDD
1,2,3,6,7,8-HxCDD
1,2,3,7,8,9-HxCDD
1,2,3,4,6,7,8-HpCDD
1,2,3,4,6,7,8,9-OCDD
TOTAL PCDD
2,3,7,8-TCDF
1,2,3,7,8-PeCDF
2,3,4,7,8-PeCDF
1,2,3,4,7,8-HxCDF
1,2,3,6,7,8-HxCDF
2,3,4,6,7,8-HxCDF
1,2,3,7,8,9-HxCDF
1,2,3,4,6,7,8-HpCDF
1,2,3,4,7,8,9-HpCDF
1,2,3,4,6,7,8,9-OCDF
TOTAL PCDF
Amt(B$
0.01
0.008
0.03
0.02
0.02
0.04
0.34
0.04
0.01
0.01
0.03
0.008
0.01
0.02
0.03
0.03
0.06
Total
X
X
X
X
X
X
X
X
X
X
X
X
X
X
X
X
X
EPA TEFs,
TS?
1
0.5
0.1
0.1
0.1
0.01
0.001
0.1
0.05
0.5
0.1
0.1
0.1
0.1
0.01
0.01
0.001
1989 a: 0.0387 ng
Equivalent
0.01
0.004
0.003
0.002
0.002
0.0004
0.00034
0.0217
0.004
0.0005
0.005
0.003
0.0008
0.001
0.002
0.0003
0.0003
0.00006
0.017
Page 1 of 1
TEFFR vS.08, LARS 6.08.00
Triangle Laboratories, Inc.®
801 Capitola Drive • Durham, North Carolina 27713
Phone: (919) 544-5729 • Fax: (919) 544-5491
Printed: 16:22 11/11/96
2G1
-------
Initial
Data Review By:
..Date..
Calculated Noise Area:
3.40
The Total Area for each peak with an ion abundance ratio outside
ratio limits has been recalculated according to method requirements.
Page No,
11/11/96
Listing of T966612B.dbf
Matched GC Peaks / Ratio / Set. Time
Compound/
M_Z.... QC.Log Omit Why ..RT. OK Ratio Total.Area... Area.Peak.1.. Area.Peak.2.. Rel.RT Compound.Name.. ID.
TCDF
304-306 DC NL 0
13
13
13
13
14
H 14
14
D D cb 14
M 15
15
M 15
15
16
« 16
DC SH 16
0.
:00 SO
:07 RO
:27
;37
:53
:05
:26
:42
:55
:02
:14
:28 RO
:40
:06
:20 RO
:35 RO
65-0.89
1
1
0
0
0
0
0
0
0
0
0
1
0
0
0
3
.26
.03
.79
.74
.85
.82
.81
.78
.80
.79
.82
.02
.89
.80
.63
.37
304-306 13 Peaks
13C12-TCDF
316-318 DC NL 0
14
14
15
15
15
16
DC WH 17
DC WH 18
0,
:00 RO
:40
:55
:13
:37
t51
:05 RO
:37 RO
:01 RO
3
67
43
34
191
137
98
87
81
142
33
28
109
24
11
0
1,008
.36
.47
.45
.27
.49
.29
.80
.39
.45
.50
.14
.14
.20
.49
.33
.96
.96
39
19
14
87
61
44
38
62
14
16
51
10
4
.45
.18
.58
.86
.80
.30
.41
.80
.91
.20
.37
.86
.93
38
24
19
103
75
54
48
79
18
15
57
13
7
,65-0.89
0
0
0
0
0
0
0
0
0
.98
.77
.68
.84
.75
.86
.59
.33
.53
316-318 6 Peaks
3
36
4
19
5,689
9
42
4
2
5,802
.18
.75
.87
.18
.90
.53
.72
.37
.09
.95
15
1
8
2,432
4
18
.93
.97
.74
.69
.41
.58
20
2
10
3,257
5
31
0.
.12
.27
.69
.63
.49
.50
.98
.70
.23
.90
.83
.63
.87
0.
.82
.90
.44
.21
.12
.50
828-1.138
0
0
0
0
0
0
0
0
0
0
0
0
1
1
1
1
.000
.840
.861
.872
.889
.902
.924
.941
.955
.963
.975
.990
.003 2378-TCDF AN
.031
.046
.062
936-1.064
0
0
0
0
1
1
1
1
1
.000
.939
.955
.974
.000 13C12-2378-TCDF ISO
.015
.030
.128
.154
Above: TCDF / TCDD Follows
TCDD
320-322
DC NL
DC SN
0
14
14
14
15
15
15
16
16
16
:00
:03
:21
:35
:12
:26
:52
:12
:18
:36
0,
RO
RO
RO
RO
,65-0.89
2
0
0
0
0
0
0
0
0
1
.15
.84
.74
.41
.77
.73
.50
.76
.74
.37
1
202
106
4
63
.04
.09
.18
.51
.35
14.07
6
10
24
2
.14
.13
.07
.16
92
45
1
27
5
2
4
10
.06
.13
.96
.51
.92
.67
.38
.26
0.846-1.086
0.000
110.03 0.856
61.05
4.81
35.84
8.15
5.30
5.75
13.81
0.874
0.888
0.926
0.940
0.966
0.987
0.993
1.011
Triangle Laboratories, Inc.® Analytical Services Division
801 Capitals Drive • Durham, North Carolina 27713
Phone: (919) 544-5729 • Fax: (919) 544-5491
Printed: 15:5411/11/96
20 2
-------
Page No.
11/11/96
Listing of T966612B.db£
Hatched GC Peaks / Ratio / Ret. Time
Confound/
M_2 QC.Log Omit Why ..RT. OK Ratio Total.Area Area.Peak.1.. Area.Peak.2.. Rel.RT Compound.Name.. ID.
320-322
37C1-TCDD
328
328
13C12-TCDD
332-334
N
332-334
PeCDF
340-342
M
D
D
A
D
D
D
M
D
D
DC
DC
DC
DC .
DC
DC
DC
DC
DC
DC
DC
DC
DC
DC
DC
DC
DC
DC
DC
D
D
DC
D
D
D
DC
D
D
SN
SN
WH
WH
WH
8
NL
WL
WL
WL
3
NL
SN
SN
4
NL
SN
SN
SN
SN
SN
SN
SN
SN
SN
SN
SN
SN
SN
SN
SN
17:13
17:31
17:50
17:54
18:05
Peaks
0:00
13:59
14:13
14:20
15:00
16:26
16:55
Peaks
0:00
15:11
16:11
16:25
16:48
'17:03
17:09
Peaks
0:00
18:02
18:22
18:59
19:04
19:10
19:19
19:32
19:43
19:57
20:06
20:11
20:16
20:30
20:39
20:48
20:53
21:08
21:18
21:43
21:52
22:03
RO
RO
RO
RO
RO
0.
RO
RO
1.
1.
5.
0.
1.
65-
63
SO
69
45
10
2
2
-0.89
2.42
0.
,60
0.78 3
0.78 4
RO
RO
RO
1.
RO
RO
RO
RO
RO
RO
RO
RO
RO
RO
RO
RO
RO
RO
RO
RO
RO
0.54
0.27
4.75
8
71 "U.^, »« .
1.
1.
0.
0.
0.
430.
0.
1.
2.
2.
40.
,854.
4.
,898.
04
52
28
98
35
54
61
39
16
69
61 40.61
18 2,854.18
02 4.02
81
1.
1.
1.
1.
1.
0.878-
0.
0.
0.
0.
0.
1.
1.
049
067
085
090
102
•1.122
ooo
852
866
873
914
001 37C1-TCDD
,030
SUR1
0.878-1.122
2.
14.
,476,
.67
,80 6.44
.03 1,518.13
,595.90 2,010.49
47.16 20.51
2.85
0.85
0.000
10.66 0,
1,957.90 0.
2,585.41 1.
38.00 1.
1
1
.925
.986 13C12-1234-TCDD
.000 13C12-2378-TCDD
.023
.039
.045
RSI
IS1
,133.89
32-1.78
0
1
0
0
0
1
0
1
1
1
0
0
0
1
0
1
1
0
1
0
2
2
.34
.45
.24
.45
.14
.27
.31
.75
.59
.51
.72
.81
.83
.45
.53
.13
.90
.60
.21
.53
.02
.57
0
40
0
0
0
0
0
16
66
1.6
0
3
3
29
0
12
8
5
12
1
8
6
J 1 Kt£\~UE X^J J* ,LWW=>
.49
.74 24.13
.43
.81
.26
.92
.90
.67 10.60
.74 41.02
.29 9.81
.38
.57
.04
.40 17.40
.58
.50
.11
.71
.73 7.74
.01
.26
.32
0.855-1.112
0
16.61 0
0
0
0
0
0
6.07 0
25.72 0
6.48 0
0
0
0
12.00 0
0
0
1
1
6.39 1
1
1
1
.000
.864
.879
.909
.913
.918
.925
.935
.944
.955
.962
.966
.970
.982
.989
.996
.000 12378-PaCDF
.012
.020
.040
.047 23478-PeCDF
.056
AN
AN
Triangle Laboratories, Inc.® Analytical Services Division
801 Capitola Drive * Durham, North Carolina 27713
Phone: (919) 544-5729 • Fax: (919) 544-5491
Printed: 15:54 11/11/96
2G3
-------
Page No.
11/11/96
Listing o£ T966612B.db£
Matched GC Peaks / Ratio / Ret. Time
Compound/
H_Z.... QC.Log omit Why ..RT. OK Ratio Total.Area... Area.Peak.1.. Area.Peak,2.. Rel.RT Compound.Name.. ID,
340-342
13C12-P6CDF
352-354
352-354
PeCDD
356-358
D
M
356-358
13C12 -PeCDD
368-370
368-370
DC
DC
DC
DC
DC
DC
DC
DC
DC
DC
D
DC
DC
DC
DC
DC
DC
DC
DC
DC
DC
DC
SN
SN
SN
SN
WH
WH
6
NL
SN
9
NL
SN
SN
SN
SN
SN
SN
SN
SN
WH
WH
WH
5
NL
SN
4
22:12
22:25
22:36
23:02
23:16
23:33
Peaks
0:00
19:41
20:25
20:53
21:07
21:17
21:29
21:52
22:11
22:22
23:01
Peaks
0
19
20
21
21
21
21
22
22
:00
:58
:56
:08
:22
:43
:58
:11
:22
22:26
22
22
22
22
23
23
23
:32
:44
:50
:54
:14
:17
:27
RO
RO
RO
RO
RO
1.
RO
RO
RO
RO
RO
RO
RO
1.
RO
RO
RO
RO
RO
RO
RO
RO
RO
RO
RO
RO
RO
0.61 0.61
2.43 1.17
0.50 1.15
4.39 0.97
0.05 0.95
1.41 1.11
182.57
32-1.78
0.13 0.12
1.00 11.95 7.26
1.24 10.35 6.29
1.45 4,741.33 2,803.80
0.71 16.44 9.98
3.14 7.98 9.82
1.94 1.96
1.41 2,961.94 1,732.50
1.16 5.30 3.22
1.74 4.52 2.87
1.67 5.13 3.21
7,764.94
32-1.78
1.46 1.28
1.27 63.56 38.62
1.64 34.80 21.63
9.38 1.40
2.22 16.04 13.97
0
1
0
0
0
2
3
4
0
7
4
1
.86
.61
.42
.94
.23
.69
.30
.20
.64
.38
.83
.34
Peaks
0
21
22
22
22
22
-.00
:39
:20
:30
:47
-.56
1.
RO
RO
RO
RO
3
15
0
3
0
1
0
0
1
0
0
1
133
.09
.52 9.58
.73
.54 2.15
.34
.78
.26
.38
.80
.20
.31
.92
.46
.32-1.78
10
2
1
1
1
0
.75
.05
.49
.63
.08
.77
Peaks
0
1
2,787
279
2
5
3,075
.10
.58
.45 1,668.49
.45 173.01 ,
.52 1,53
.98 3.65
.40
1.063
1.073
1.082
1.103
1.114
1.128
0.808-1.192
0.000
7.27 0.943
5.08 0.978
1,937.53 1.000 13C12-PeCDF 123 IS2
14.09 1.011
3,13 1.019
1.029
1,229.44 1.047 13C12-PeCDF 234 SUR2
2.78 1.062
1.65 1.071
1.92 1.102
0.885-1.034
0.000
30.43 0.894
13.17 0.937
0.946
6.29 0.957
0
5.94 0
0
2.29 1
1
1
1
1
1
1
1
1
.972
.984
.993
.001 12378-PeCDD AN
.004
.009
.018
.022
.025
.040
.043
.050
0.821-1.179
0
0
1,118.96 1
106.44 1
1.42 1
4,71 1
,000
.969
.000 13C12-PeCDD 123 IS3
.007
.020
.027
Triangle Laboratories, Inc.® Analytical Services Division
801 Captela Drive • Durham, North Carolina 27713
Phone: (919) 544-5729 « Fax: (919) 544-5491
Printed: 15:5411/11/96
2G4
-------
Page No.
11/11/96
Listing of T966612B.dbf
Hatched GC Peaks / Ratio / Set. Time
Compound/
M_Z.... QC.Log omit Why ..BT. OK Ratio Total.Area— Area.Peak.1.. Area.Peak.2,. Rel.RT Compound.Name.. ID.
HxCDF
374-376
M
H
M
M
M
374-376
13C12-HXCDF
384-386
DC
DC
DC
DC
DC
DC
DC
DC
DC
DC
NL
SN
SN
SN
SN
SN
SN
SN
SN
5
NL
0:
24:
24:
24:
25:
25:
25:
25:
25:
25:
26:
26:
26:
26:
00
08
18
38
15
23
29
33
38
58
01
02
31
49
1.
RO
RO
RO
RO
RO
RO
RO
RO
RO
Aoove : r&t-LJV / njo-wr rw4-j.owt> — -
05-1.43
1.
1.
1.
0.
1.
1.
0.
1.
0.
1.
1.
2.
0.
1 .
37
19
53
79
43
31
76
63
90
45
78
,14
,58
,18
Peaks
0:
00
0.
RO
24:08
24:17
RO
25:15
25:21
25:57
DC
SN
26:11
RO
26:42 .
384-386
HxCDD
390-392
D
M
M
DC
D
DC
DC
DC
DC
DC
DC
7
NL
SN
SN
SN
SN
SN
SN
WH
26:
;53
RO
2.
8.
13.
1.
12.
5.
1.
0.
0.
5.
0.
46
89 4.83
53 9.23
55
50 7.35
12 2.90
23
43
83
08 3.30
40
0.49
1.
0.
45.
,21
.85
,12
43-0.59
1.
0.
.10
.52
0.40
0
0
0
0
0
0
.48
.48
.48
.27
.47
.24
Peaks
0
24
25
25
25
25
25
25
26
26
:00
:46
:17
:26
:31
:37
:43
:56
:38
:44
1,
RO
RO
RO
RO
RO
RO
RO
RO
RO
1.84
12,
8,
2,365,
3,635
2,261
1
2,020
5
10,309
: HxCDi
.22 4.19
.76 2.95
.34 768.07
.63 1,182.39
.50 732.22
.74
.76 647.72
.03 1.69
.24
F/ Wvf^TM"* 'S/^l l CM^C «• •<—
/ ttXX- LJlJ £ O J. 4.Q wS ~ ~"
.05-1.43
0
1
1
0
0
0
0
1
0
2
.78
.47
.07
.51
.99
.39
.91
.78
.91
.25
1
3
43
0
7
0
0
1
0
0
.77
.54
.10 22.30
.36
.73 4.28
.83
.92
.43
.36
.36
0.945-1.064
0.000
4.06 0.952
6.04 0.959
0.972
5.15 0.996 123478-HxCDF
2.22 1.001 123678-HXCDF
1.005
1.008
1.011
2.27 1.024 234678-HxCDF
1.026
1.027
1.046
1.058
0.842-1.158
0.000
8.03 0.952
7.40 0.958
1,597.27 0.996 13C12-HXCDF 478
2,453.24 1.000 13C12-HXCDF 678
1,529.28 1.024 13C12-HXCDF 234
1.033
1,373.04 1.053 13C12 -HxCDF 789
7.09 1.060
0.939-1.017
0.000
0.946
20.80 0.966
0.971
4.33 0.975
0.978
0.982
0.990
1.017
1.021
AN
AN
AN
SDR3
1S4
ALT2
ALT1
390-392
13C12-HxCDD
402-404
2 Peaks
1.05-1.43
DC NL 0:00 RO 1.75
1.21
1.23
1.23
25:31
26:06
26:11
26:22
1.18
50.83
1.68
7.50
1,550.28
2,784.18
12.36
0.962-1.038
0.000
4.10 3.40 0.975
855.54 694,74 0.997 13C12-HXCDD 478 SUR4
1,537.05 1,247.13 1.000 13C12-HXCDD 678 IS5
6.68 5.68 1.007
Triangle Laboratories, Inc.® Analytical Services Division
801 Caprtola Drive » Durham, North Carolina 27713
Phone: (919) 544-5729 • Fax: (919) 544-5491
Printed: 15:54 11/11/96
O r r
.•- 0 J
-------
Page No.
11/11/96
Listing of T966612B.dfcf
Matched GC Peaks / Eatio / Ret. Time
Compound/
M_Z.... QC.Log Omit Why . .RT. OK Ratio Total.Area— Area.Peak.1.. Area.Peak,2.. Rel.RT Conpound.Narae.. ID.,
402-404
HpCDF
408-410
H
408-410
13C12 -HpCDF
418-420
418-420
26:30
26:42
2,6:47
26:49
DC SN 26:51
8 Peaks
DC NL 0
28
DC SN 28
DC SN 29
DC SN 29
DC SN 29
DC SN 29
DC WH 29
:00
:20
:28
:OS
:14
:30
:37
:47
RO
RO
RO
RO
0.
RO
RO
RO
RO
RO
RO
RO
1
0
1
0
0
.26 2,092
.89 4
.88 4
.92 3
.99 1
6,459
,88-1.20
1
0
1
3
2
1
2
1
.55
.95
.90
.90
.44
.90
.54
.89
1 Peak
DC NL 0
28
29
29
:00
:19
:35
:50
0,
RO
RO
1
13
0
0
0
0
1
0
13
.46
.56
.50
.25
.64
.09
T"l / MTV""*
u i rijx.
.31
.42
.84
.20
.51
.59
.47
.71
.42
,37-0.51
0
0
0
0
.91
.40
.40
.92
3 Peaks
2
2,301
1,159
2
3,463
•o • «*^/Ti
.48
.75
.10
.84
.69
17 / 5frv~
1,166.99 925.47 1
2.53 2.83 1
3.77 2.01 1
1.80 1.96 1
1
.012 13C12-HXCDD 789
.020
.023
.024
.025
RS2
0.995-1.051
0
6.54 6.88 1
1
1
1
1
1
1
0.929
0
654.68 1,647.07 1
330.62 828.48 1
1.82 1.97 1
.000
.001 1234678-HpCDF
.005
.027
.032
.042
.046
.052
-1.141
.000
.000 13C12 -HpCDF 678
.045 13Cl2-HpCDF 789
.054
AN
IS6
SCTR5
HpCDD
424-426
424-426
13C12 -HpCDD
436-438
436-438
DC NL 0 : 00
28:38
29:16
2 Peaks
DC NL 0:00
28:36
29:15
2 Peaks
0.
RO
RO
88-1.20
1
1
1
.59
.75
.16
1,
5
11,
.20
.02
.46
4.30
6.16
16.48
0.
RO
RO
,88-1.20
1
1
1
.23
.81
.00
2
2
2,293
2,296
•ft , tlw—TYl
.57
.90
.11
.01
™\ / r\f
2.57
1,144.75
0.973-1.006
0.000
2.46 0.979
5.30 1.001 1234678-HpCDD AN
0.966-1.034
0.000
1.42 0.978
1,148.36 1.000 13C12-HpCDD 678 IS7
OCDF
442-444
442-444
OCDD
458-460
458-460
0.76-1.02
DC NL 0:00 RO 1.11
31:48 0.95
1 Peak
0.76-1.02
DC NL 0:00 RO 0.51
31:44 RO 0.63
1 Peak
2.08
11.00
11.00
0.62
55.21
55.21
5.36
26.00
0.874-1.126
0.000
5.64 1.003 OCDF
0.874-1.126
0.000
41.20 1.001 OCDD
AN
AN
Triangle Laboratories, Inc.® Analytical Services Division
801 Capitola Drive « Durham, North Carolina 27713
Phone: (919) 544-5729 » Fax: (919) 544-5491
Printed: 15:54 11/11/96
r
b
-------
Page No.
11/11/96
Listing of T966612B.dfa£
Matched GC Peaks / Ratio / Ret. Time
Compound/
M_Z.... QC.Log Omit Why ..RT. OK Ratio Total.Area... Area.Peak.1.. Area.Peak.2.. Rel.RT Compound.Name.. ID.,
13C12-OCBD 0.76-1.02
470-472 DC NL 0:00 1.00 0,06
31:43 0.91 2,573.81
470-472 1 Peak 2,573.81
1,227.77
0.995-1.006
0.000
1,346.04 1.000 13C12-OCDD
IS8
Column Description "Why" Code Description QC Log Desc.
M_Z -Nominal Ion Mass(es)
..RT. -Retention Time (mm:ss)
Rat.l -Ratio of M/M+2 Ions
OK -RO=Ratio Outside Limits
Rel.RT-Relative Retention Time
End of Report
WL-Below Retention Time Window
WH-Above Retention Time Window
SN-Below Signal to Noise Level
-------
?ile:T966612 #1-835 Acq:l-NOV-96 07:30:16 EI+ Voltage SIR 70T
519.8965 F:2 Exp:EPCUS
Sample Text:23B-3 TLI #39291R1 INJ. TIME =
501
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File:T966612 #1-835 Acq:l-NOV-96 07:30:16 EI+ Voltage SIR 70T
321.8936 F:2 Exp:EPCUS
Sample Text:23B-3 TLI #39291R1 INJ, TIME = 07:32 File Text:231-3 TLI #»
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331.9368 F:2 Exp:EPCUS
Sample Text:23B-3 TLI #3929lRl INJ. TIME = 07:32 File Text:23B-3 TLI #»
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-------
File:T966612 #1-835 Acqil-NOV-96 07:30:16 EI+ Voltage SIR 70T Noiaeill93
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TRIANGLE LABS Teit:23B-3 TLI #39291R1 • INJ. TIME = 07:32
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305.8987 F:2 BSUB(256, 30,-3 .0 ) PKD( 5,3,1, 0.101,3808. 0, 0. 00%, F,F) Exp-.EPCUS
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TSIANGLE LABS Text:23B-3 TLI #39291S1 INJ. TIME = 07:32
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317.9389 F:2 BSUB(256, 30,-3 .0 ) PKD(5, 3,1, 0.10%, 3556. 0, 0. 00%, F, F) Exp:EPCUS
TRIANGLE LABS Text:23B-3 TLI #39291R1 INJ. TIME = 07:32
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TRIANGLE LABS Text:23B-3 TLI #39291R1 ZK7. TIME =
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80:
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File:T966612 #1-835 Acq:l-NOV-96 07:30:16 EI+ Voltage SIR 70T
375.8364 F:2 Exp:EPCUS
TRIANGLE LABS Teit:23B-3 TLI #39291R1 INJ. TIME = 07:32
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2.2E5
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18:00 Time
5. 9E6
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18:00 Time
7.6E6
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14:00
1500
1600
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18:00 Time
-------
File:T966612 #1-835 Acq: l-NOV-96 07:30:16 EH- Voltage SIX 70T Noise: 636
319.8965
Fs2 BSOB(256,30r-3.0) PXD(5,3,l,0.10*f2544.0,0.00%,F,F) Elp.-JSJPCDS
TRIANGLE LABS Text:23B-3 TLI #39291X1 IKT. TIKE - 07:32
100*
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00 ' ' ' ' 15-00 ' ' 16.-00 ' 17:00 ' ' 18sOO Time
FileiT966612 #1-835 Acqsl-SDV-96 07:30:16 EI+ Voltage SIR 70T Noise:295
321.8936 F:2 BSUB(256, 30, -3 .0 ) PXD(5,3,1, 0.101,1180. 0, 0. 00%,F,F) RtpsXPCOS
TRIANGLE LABS Text i 238-3 TLI #39291X1 IKT. TIME = 07:32
100*
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00 ' ' ' ' ' 15:00 ' IgioO 171-00 ' ISsOO Time
File:T966612 #1-835 Acq:l-NOV-96 07:30:16 EI+ Voltage SIX 701 Noise:1831
331.9366 f:2 BSUB(256, 30, -3 .0) PKS(5, J, 1,5. 10%, 7324 ,0,0. 00%, F,F) Exp;EPCUS
TRIANGLE LABS Text:23B-3 TLI #39291X1 JMT. TIME = 07:32
1004
sol
60:
401
20:
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14:
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File:T966612 #1-835 Acq:l-NOV-96 07:30:16 EI+ Voltage SIX 70T Noise: 756
333.9338 F:2 BSVB(256,30,-3 .0) PXD(5, 3, 1,0. 101,3024. 0,0.00*,F,F) Exp:EPCUS
TRIANGLE LABS Text:23B-3 TLI #39291X1 IW. TIME = 07:32
loos
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40:
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0:
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Tile:T966612 #1-835 Acq:l-NOV-96 07:30:16 XI + Voltage SIR 701 lToise:304
327,8847 F:2 BSUB(256, 30, -3 .0 } PXD(5, 3,1, 0.10%,1216. 0, 0. 00\,F ,F) ExpsEPCUS
TRIANGLE LABS Text:23B-3 TLI #39291X1 Illy. TIME - 07:32
IOCS
aol
601
401
20:
o-
14-
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1
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00 15:00 16:00 17:00 18:00 Tiae
File:T966612 #1-835 Acq:l-SOV-96 07:30:16 XI + Voltage SIX 70T
330.9792 F-.2 ExpsEPCUS
TSIAHSLE LABS Text: 238-3 TLI #39291X1 IKT. TIME = 07:32
1003
80l
601
40:
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14:00 15.-00 16:00 17sOO 18:00 Time
270
-------
'ileiT9S6612 #1-835 Aoqil-SOV-96 07:30:16 EI+ Voltage SIR 70T Soiae:14$
39.8597 F:2 BSUS(256,30,-3.0) PKD(5r3,1, 0.10\,S96.0,0.00*, f,f) ExpiEFCUS
TRIANGLE LABS Text:23B-3 TLI $39391X1 JJKT. TIME - 07:32
lOOi A4.10E5
18:00 19:00 20:00 21:00 22:00
File:T966612 #1-835 Acqsl-NOV-96 07s30sl6 EI+ Voltage SIR 70T Noiae:445
341.85S7 F:2 BSOBfSSS, JO, -3.0) PKS(5,3,1, 0.10^,1780.0,0. 00*,F,F) ExpsEPCUS
TRIASSLS LABS Text:23S-3 IXI #39291X1 IK7. TIME - 07:32
100* A2.57S5
60
40:
20:
ol
A2.41ES
Al.68E4
AI . a ess
A7.60S4 A5.61S4
A6.B6K3
20
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6.48E4
2.69S4
A5.77E4
18:00 19:00 20:00 21:00 22:00
F±lesT966612 #1-835 Acg:l-NOV-96 07:30:16 EI+ Voltage SIR 70T Koiae:34
351.9000 F:2 BSUB(25G,30, -3.0) PKD(5 , 3,1,0.10%, 136.0, 0.00\,F,F) Exp:EPCUS
TRIANGLE LASS Text:23S-3 TZI #39291X1 IKJ. TIME - 07:32
1004 A2.80E7
802
60:
401
20:
o:
Al. 73E7
18:00 15:00 20;r 00 21:00 22:00
File:T966612 #1-835 Acq:l-NOV-96 07:30:16 Eli- Voltage SIS 70T Noiae:269
353.8970 F:2 BSU3(256,30,-3.0) PKD(5,3,1, 0.10%, 1076.0, 0. 00%,F,F) ExpsEPCUS
TRIANGLE LABS Text:23B-3 TX.I #3S291R1 I1KT. TIME =• 07:32
IOCS
40.
20.
0. _
'l8«00 19.-00 20:00 21iOO
File:T966612 #1-835 Acq:l-NOV-96 07.-JO.-1S EH- Voltage SIR 70T
330.9792 F:2 Exp:EPCUS
TRIANGLE LABS Text:23B-3 TLI #39291R1 INJ. TIME •
100% 18!2JMLllJ>$!59 1SJ.56 20:16 20.30 21s 13 21-38
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18:00 19:00 20:00 21:00 22:00
File:T966612 #1-835 Acqsl-NOV-96 07:30:16 EI+ Voltage SIS 70T
409.7974 F:2 ExpsEPCUS
TRIANGLE LABS Textt23B-3 TLI #39291R1 IJKT. TIME " 07:32
23: 00
23:00
23:00
23:00
23:02
23:00
-7.1E4
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Time
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.3.9E6
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Time
4.5E6
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2.7E6
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9.1E5
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.2.6E7
.2.1E7
.1. 5E7
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19:00
20:00
21100
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23:00
271
-------
FTLesT96eS12 11-335 Acq":l-Nbv-9S 07:30:16 E±+ VSItagre SIS 70* Noiae:37S
355,8546 F:2 BSOB(256,30,-3.0) PKD(5, 3, 1, 0.10%,1515. 0,0.00%, r,F) ExptEPCOS
TKIAmiLE LABS Teits23B-3 TLI #39291X1 - IIU. TIME » 07:32
1004
so:
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401
201
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A3 . 86E5
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File:T96S612 #1-835 Acqsl-NOV-96 07:30:16 EI+ Voltage SIR 70T Noiaes2Sl
357.8516 Fs2 BSVS(256,3Q,-3.0) PXD(5,3,1, 0.101,1044.0,0 . 00%, Jf,F ) Exp:EPCUS
TXIANGLE LABS Text:23B-3 TLI #392S1X1 XH57. TIME = 07(32
1004
so:
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401
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20;
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20:00 21-00 221-00
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23:00 ' Tine
File:T966612 #1-835 Acq:l-KOV-96 07:30:16 EH- Voltage SIS JOT «oise:217
367.8949 F:2 BSOB(256, 30, -3 .0) PKD(5, 3,1, 0.10%, 8S8, 0, 0. 00%,F,F,> Elp:EPCVS
TRIANGLE LABS Text:23B-3 TLI #392913.1 IWJ, TIME = 07:32
loos
so:
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401
201
•
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23 1 00 Time
File:l'S6SS12 #1-835 Acq:l-KOV-96 07:30:16 EI+ Voltage SIS 70T Noiae:20
369.3919 F:2 BSUB(256, 30, -3. 0) PKD(5,3,1, 0.10%, 80. 0, 0. 00%,F,F; Exp:EPCUS
TRIAHSLE LABS Text:23B-3 TLI #39291X1 IKJ". TIKE = 07:32
1005
aoi
601
401
20.
0'
A1'\
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20:00 ' ' ' 21:00 ' ' ' ' 22.- 00
File:T966612 #1-835 Acq:l-NOV-96 07.-30.-1S El* Voltage SIS 70T
330.9792 f:2 ExpiEPCUS
12S7
Al . 06E6
X/v
-2.SE6
12.2E6
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15 . 5£5
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23 s 00 Time
TRIASSLE LABS Text:23B-3 TLI #39291S1 JJKT. TIME = 07:32
1003
80.
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40.
20.
0
*^t^~^¥j&3t^^^~^^^ 21° 5* 22:11
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212
-------
File:TSS6612 #1-505 Acysl-NOV-96 07i30slS EI+ Voltage SIR TOT Noiaes710
73.8208 F:3 BSVB(256,30,-3.0) KED(5,J,1,0.10*,2940.0,0.00*,?,F) ExpsEPCUS
TRIANGLE LABS Text:23B-3 TLI #39291S1 XMJ. TIME » 07s 32
1004 A7.99E4
24s00 25:00 26:00
FileiT9S$S12 fl-505 Acq:l-NOV-96 07s30:lS EI+ Voltage SIS 70T Noiae:520
375.817S F:3 B£V3(256,30r -3.0) ?XS(Sf 3,leO.101,2080.0,0. 00\,f,F) BxpsEfCUS
TRIANGLE LASS Text:23B-3 TLI #39291M1 IJKT. TIME = 07:32
1003j A5.33E4
Al.88E4
A6.71E31 A4.S5E3
27s 00
24:00 25:00 26:00
File:T966612 #1-505 Acc[il-NOV-96 07:30:16 EH- Voltage SIM 70T Noise: 670
383.8639 F:3 BSOB(256,30, -3.0) fXD(5,3,1,0.10^,2680.0,0, 00%,T,t) Exp:EPCUS
TRIANGLE LABS Text:23B-3 TLI #39291X1 MET. TIME = 07:32
1003,
to;
201
24:00 25:00 26:00
File .-19 66612 #1-505 Acq:l-NOV-96 07:30:16 EI+ Voltage SIS 70T Noiaet612
385.8610 F:3 8503(256, 30, -3. 0) PKZ>(5,3,1, 0,101,2448.0,0.001,F,F) Exp:EPCUS
TRIANSLE LASS Text:23B-3 TLI 039291M1 IJK7. TIME = 07:32
10 OS A2.45E7
27:00
ill
*7't2ES A6.4SE6
\ l\ !\
27:00
80;
sol
40;
20;
A1.53E7
A1.37E7
24s00 25:00 26:00
F±le:T966612 #1-505 Acq:l-NOV-96 07:30:16 EI+ Voltage SIS 70T
392.9760 F:3 Exp-.EPCUS
TRIANGLE LABS Text:233-3 TLI #39291M1 INJ. TIME
""W^twv^av^^^9 25:0i - ~-2**25 2Sl47 26:1°
ao;
60;
40;
20;
01
27: 00
3.5E6
2.BE6
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7.1E5
O.OEO
Time
.7.4E6
.6.0E6
.4.5E6
.3. OE6
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Eune
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.2.5E6
24:00 25:00 26:00
File:T966612 #1-505 Acq:l-NOV-96 07:30:16 EH- Voltage SIX 70T
445.7555 F:3 ExpsEPCUS
TRIANSLE LABS Text:23B-3 TLI §39291M1 JMJ. TIME -
2Sr-ll
27:00
.O.OEO
Time
07:32
24:00
25:00
25s 00
27:00
273
-------
'File:~T966Sl2 il-SOS Acqil-N0V-96 07s30:lS tt+ Voltage S±J» ?OT Ho±fet451
389.8156 F:3 BSU3(256, 30, -3. 0) PKD(5,3,1,0.10%,1964.0,0.00*^,1-) Exp:EPCVS
TRIANGLE LABS Text:23B~3 TLI #39291S1 IXJ", TIME =• 07:32
1004 A2.Q8E5
24:36 24:48 25:00 25:12 25:24 25:36 25:48 26:00 26:12 26:24 26:36 26:48
FilesT966612 #1-505 Acq:l-SOV-96 07:30:16 EH- Voltage SIS 70T Noises626
391.8127 F: 3 BSDB(256 ,30,-3 .0 ) PKS(5, 3,1, 0.101,2504 . 0, 0. 00%,F, F) ExpiEPCUS
TRIANGLE LABS Texts23B-3 TLI #39291R1 IJKT, TIME - 07:32
1003, A2.01E5
so:
eo:
24:36 24:48 25:00 25:12 25:24 25:36 25:48 26:00 26:12 26:24
File:T966612 #1-505 Acqsl-WOV-96 07:30:16 Eli- Voltage SIR 70T Noises654
401.8558 F:3 BSUB(2S6,30,-3.0} PKD(5,3,1, 0.10%,2616. 0,0. 00%,F,F) Exp:EPCUS
TXIANGLE LASS Text:23S-3 TLI #39291111 XXI. TIME = 07:32
100* A1.5.4S7
40:
20.
A4.47E4
Al.58E4
26t36 26:48
so:
so:
40:
20:
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24:36 24:48 25:00 25:12 25:24 25:36 25:48 26:00 26:12 26:24 26:36 26:48
File:T966612 #1-505 Acq:l-NOV~96 07:30:16 EI+ Voltage SIS 701 Noiae:373
403.8529 F:3 SSVB(256, 30, -3. 0) PKD(5,3,1, 0.10%, 1492. 0, 0. 00%,r,T) Elf.EFCOS
TRIANGLE LABS Tejct:23B-3 TLI #39291X1 JWJ. TIME - 07:32
1003, A1.25E7
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40.
20:
A6.95E
A9.25E6
24:36 24:48 25:00 25:12 25:24 25:36 25:48 26:00 26:12 26i24 26:36 26:48
File:T966612 #1-505 Acg:l-NOV-96 07:30:16 EI+ Voltage SIS 70T
392.9760 F:3 Exp-.EPCaS
TRIANGLE LABS Teit:23S-3 TLI #39291X1 IKT. TIME = 07:32
1003
BO:
SO.
40:
20:
0.
24:49
26:10
26:37 26:47
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Time
.4. 5E6
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Time
.3. 8E6
.3. OE6
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Time
.1. 3E7
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24:36 24:48 25:00 25:12 35:24 25s36 25i48 26tOO 26-12 26:24 26:36 26s4S
O.OEO
Time
274
-------
FilesT966612 #1-443 Acq:l-HOV-96 07:30:16
407.7818 F.-4 BSUB(256,30, -3.0) PKD(S,3,1,0
TRIANGLE LABS Texts 23B-3 TLI #39291X1
100S
80J
60:
40:
201
O'
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A4 . 19E4
/V A6.80E3
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28:12 ' ' ' 28:24 ' ' ' 28:36 ' ' 28^48
EJ* Voltaye SIS 70T Noise: 4 94
. 101,1976. 0,0. 00%,F,F; ExpsEPCOS
IWJ. TJME » 07:32
' 29:00 '
Al . 83E4
29:12' ' '29:24' .29>36'
7.8F4
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File:T966612 '#1-443 Acq:l-HOV-96 07:30:16 EH- Voltage SIS 70T Wbi*e:319
409.7789 F:4 BSUB(256,30r -3.0) PXD( 5,3,1, 0.10^,1276.0, 0.00*,F,F) Exp:EPCUS
TRIANGLE LABS Texts23B-3 TLI #39291X1 JK7. TIME = 07:32
1003
aol
601
40:
201
A6.72E4
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28:12 28:24 28:36 28:48
' 29:00 '
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29:48' ' 30:00
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Time
File .-1966612 #1-443 Acqil-NOV-96 07:30:16 EI+ Voltage SIX 70T Soism:783
417.8253 F:4 BSUB(256, 30, -3 .0) PXD( 5, 3,1, 0.10%,3132. 0,0 . 00*,F,F) Exp:EPCUS
TRIANGLE LABS Text;23B-3 TLI #39291X1 JKT. TIKE " 07:32
1001
80J
601
40:
20:
o"
A6.55E6
A
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28:12 28:24 28:36 28:48
29:00
A3.31E6
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29:12 29:24 29s36
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29: 48 30:00
Ll . 7E6
Ll , 326
18.6E5
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Time
File:T966612 #1-443 Acq:l-KOV-96 07:30:16 EI+ Voltage SIR 70T Noiae:S59
419.8220 F:4 BSUB(256, 30, -3. 0 ) PKD(5,3,1, 0.10%, 3436. 0, 0. 00%, F,F) Sxp:EPCOS
TRIANGLE LABS Text:23B-3 TLI #39291X1 IftJ. TIKE = 07:32
1001
aol
60:
401
201
o-
Al . 65E7
n
A
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28:12 281-24 28:36 28:48
File:T966612 #1-443 Acq:l-SOV-96 07:30:16
430.9729 F:4 Exp:EPOJS
TRIANGLE LABS Tsxts23B-3 TLI' #39291X1
1003
sol
60:
40:
20:
0'
"fxJ5"^^ *8A^5s"_
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28slj' '28:24 28:36' ' ' 2Si'48 '
FileiT966612 #1-443 aegf!l-WOV-96 07:30.-16
479.7165 F:4 Exp:EPCUS
TRIANGLE LABS Texts23B-3 TLI #33291,81
100J
so:
60:
40l
20:
0"
28:16
1
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v^ L/AMAVm A'-
28:12 28:24 28:36 28:48
' 29s 00 '
EH- Voltage
28-58
s~s*^~-^~^
' 29s00
EH- Voltage
29 .-05
i L
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29:00
A8.2SE6
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29:12 29:24 29:3S
SIR 70 T
JJTJ. TIME = 07:32
>*\ ^ ^X*X»v y^X"*W"''''v. — _., _,^
jS\s~^ ™^S~ -" — ~-sXV-N-^Sx-
23:12' ' '29124' ' '29:36'
SIX 701
IWJ. TIME - 07:32
L — i jsi
w/wi/L/
23:12 23:24 23:36
5 . 5E6
' 29U'8 ' ' ' 30.' 00
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13 . 3E6
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Time
9:44 29:57
<^Ni'\^~/~«w *^~^~/-
23:48 ' ' 30:00
9.6E6
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15. 826
13.8E6
11.9E6
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Time
rl . 1E4
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-------
TLI Project: 39291rl
Client Sample: 23B-3
Method 23 TCDD/TCDF Analysis (DB-225)
Analysis File: X964238
Client Project:
Sample Matrix:
TLI ID:
Eastern Ridge Lime Facility
M23TRAIN Date Received: 10/19/96
143-23-6A-C Date Extracted: 10/21/96
Date Analyzed: 11/01/96
Spike File: SPC2NF08
KM: XF21266
ConCal: X964226
Sample Size:
Dry Weight:
GC Column:
1.000
n/a
DB-225
Dilution Factor: n/a
Blank File: T966616
Analyst: JF
% Moisture: n/a
% Lipid: n/a
% Solids: n/a
2,3,7,8-TCDF
0.04
0.65
20:23
l3C12-2,3,7,8-TCDF
5,7
71.1
40%-130%
0.79
20:22
13Ci2-l,2,3,4-TO>D
0.81
19:25
Data Reviewer:
11/11/96
Page 1 of 1
C2NF.PSR Y1.M. LARS S.W.QO
Triangle Laboratories, Inc.®
801 Cap'rtola Drive • Durham, North Carolina 27713
Phone: (919) 544-5729 • Fax: (919) 544-5491
Printed: 16:13 11/11/96
ri r> —
d J J
-------
Initial
Date...
Data Review By:
Calculated Noise Area:
7.00
The Total Area for each peak with an ion abundance ratio outside
ratio limits has been recalculated according to method requirements.
Page No. 1
11/01/96
Compound/
M_Z.... QC.Log Omit Why
Listing of X964238B.dbf
Matched GC Peaks / Ratio / Ret. Time
..RT. OK Ratio Total.Area... Area.Peak.1.. Area.Peak.2.. Rel.RT Compound.Name.. ID.
TCDF
304-306 DC NL 0:00
16:14
DC SN 16:34
DC SN 16:40
DC SN 16:49
DC SN 16:54
17:09
17:15
17:21
17:32
17;46
17:55
18:03
18:13
18:21
18:42
19:07
19:21
19:32
19:44
19:52
DC SN 20:04
DC SN 20:08
20:15
20:23
20:32
20:46
20:54
DC SN 21:10
DC SN 21:18
21:29
DC SN 22:04
DC WH 22:25
DC WH 22:32
304-306 22 Peaks
13C12-TCDF
316-318 DC NL 0:00
DC WL 19:07
DC ML 19:21
20:22
20:53
DC WH 22:08
0.
RO
RO
RO
RO
RO
RO
RO
RO
RO
RO
RO
RO
RO
RO
RO
RO
RO
RO
0.
RO
RO
RO
RO
65-0.89
0
0
1
0
0
2
0
0
0
0
0
0
0
0
1
0
0
0
0
0
0
2
1
0
0
0
0
0
0
0
0
0
1
3
.33
.85
.16
.58
.72
.61
.78
.57
.97
.91
.69
.92
.89
.81
.07
.77
.82
.83
.73
.76
.85
.06
.03
.63
.65
.67
.61
.78
.28
.82
.64
.48
'.47
.43
5.
298.
2.
6.
3.
3.
211.
181.
281.
161.
201.
202.
65.
421.
143.
468.
174.
208.
135.
43.
158.
2.
6.
126.
120.
148.
68.
116.
2.
6.
38.
11.
6.
1.
3,976.
37
59
41
71
23
95
89
83
50
83
25
36
53
30
66
80
47
07
05
73
30
55
63
18
19
21
77
44
57
20
07
67
.18
81
.02
136.
93.
79.
154.
83.
82.
105.
30.
188.
86.
203.
78.
94.
57.
18.
72.
55.
47,
59.
29.
51.
16.
78
02
37
28
40
14
15
84
69
98
86
56
64
21
95
51
15
28
32
88
01
54
161.
118.
138.
159.
91.
119.
114.
34.
232.
81.
264.
95.
113.
77.
24.
85.
86.
72.
88.
49.
65.
25.
.65-0.89
4
0
0
0
1
1
.13
.54
.83
.79
.07
.04
2.
52.
140.
23,902,
225,
263.
.10
.67
.77
.40
.19
.41
10,518,
136.
,10
,41
13,384.
126.
0.788-1.094
81
87
50
03
23
11
36
69
61
03
94
91
43
84
78
79
87
91
89
08
43
90
0.
•3.0
.95
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
1
1
1
1
1
1
1
1
1
1
.000
.797
.813
.818
.826
.830'
.842
.847
.852
.861
.872
.880
.886
.894
.901
.918
.939
.950
.959
.969
.975
.985
.989
.994
.001 2378-TCDF AN
.008
.020
.026
.039
.046
.055,
.083
.101
.106
951-1.049
0
0
0
1
1
1
.000
.939
.950
.000 13C12-2378-TCDF ISO
.025
.087
Triangle Laboratories, Inc.© Analytical Services Division
801 Caprtola Drive • Durham, North Carolina 27713
Phone: (919) 544-5729 • Fax: (919) 544-5491
Printed: 21:29 11/01/96
238
-------
Page No.
11/01/96
Listing of X964238B.dbf
Matched GC Peaks / Ratio / Ret. Time
Compound/
M_Z QC.Log Ornit Why . .RT. OK Ratio Total.Area— Area. Peak. 1.. Area. Peak, 2.. Rel.RT Compound. Name. . ID..
316-318
13C12-TCDD
332-334
2 Peaks
332-334
DC
DC
DC
DC
DC
NL
WL
SN
SN
WH
4
0.
0:00 RO
17:07 RO
18:09
19:13
19:25
19:37 RO
20:06
20:59 RO
21:43
Peaks
65-0.89
1
1
0
0
0
0
0
0
0
.19
.63
.88
.79
.81
.44
.72
.41
.76
24,127.59
Above: TCDF / TCDD Follows
0.896-1.104
1.89 0.000
4.17 0.891
62.03 29.01 33.02 0.944
16,476.99 7,289.99 9,187.00 1.000 13C12-2378-TCDD IS1
12,112.12 5,406.75 6,705.37 1.010 13C12-1234-TCDD RSI
11.53 1.021
218.80 91.81 126.99 1.046
4.12 1.092
15.53 1.130
28,869.94
Column Description "Why" Code Description QC Log Desc.
M_Z -Nominal Ion Mass(es)
. .RT. -Retention Time (mrruss)
Rat.l -Ratio of M/M+2 Ions
OK -RO=Ratio Outside Limits
Rel.RT-Relative Retention Time
End of Report
WL-Below Retention Time Window
WH-Above Retention Time Window
SN-Below Signal to Noise Level
-------
»ilo:X56433B #1-784 Acg; I-IKV-ISSS SO:41flS "OC'SI+ Voltago
303.9016 Sxp:XCQNW_TT
TOft:23B-3 TLI#39291rl File Taxt sVRXANaLE LABS
19:21
Auto'3p»c
19:00 19:12 19:24 19:36 19:48 20:00 20:12 20:24
Fil*!X964238 #1-784 Acq: l-NOV-1996 20:41:16 QC EI+ Voltaga SIR AutoSpec
305,8987 Exp:KONP_TT
Sanple Taxt:23B-3 TLI#39291rl Fila Text:TRIANGLE LABS
19:21
20:36
20:48
21 n
SSj
soj
85j
80J
75j
70J
65j
sol
55J
sol
45.
401
35.
30-
25.
202
15j
101
sl
0.
19s 07
20:16
20:33
20:54 -
2.3ES
"-2.2BS
12.1E5
12.0SS
'•.1.9SS
ll.BSS
.l.SSS
,1.525
,1. 4E5
,1.3*5
.1.2SS
ll.lSS
•-9.4E4
18.2S4
'•.7.0S4
15.9S4
"-.4.7S4
L3.SS4
L3.3S4
11.3S4
19:00
19 slS
19:48
20:00
30:12
> I 'i—i
20:24
—r-i—i—i
20i36
31
io. oso
00
233
-------
'il»iX$6423B #1-784 "Aei; "l-HoV-l99e SOillilt OC SI* Valtmg* SIR AukoSpmo
03.S01S BSm<2S6,30,-3.0} PXD{5,3,lr0.iaX,4680.0,0.00*,FrF)
T«rt.-23fl-3 TLI039291rl Fila TfartsTRIASaLS LABS
I6s00 17:00 18:00 IStOO 20:00 21tOO 22:00
'llesX964238 #1-784 Ac?.* l-NOV-1996 20tilt 16 OC SI* Voleage SIR AutoSpoc Hoisa:3533
305.8187 BSUB(256t30,-3.0) PKD{5,3,1, 0.10%, 14132.0, 0. 00*,?,P) Sup s ZCCOIF_TT
Saxpla Text:23B-3 TLI#392$lrl PH0 T«urt:TSIAWOii1 LABS
100* A2.33K6
17.-00 18.-00 19tOO 20sOO 21:00 22.-00
FilasI964238 #1-784 Acgj 1-KOV-19S6 20.-41.-1S OC EX* Voltage SIR AutoSpec Soisei24S5
315.9419 BSUB(2S6,30,-3.0} PKS{5,3,1,0.101,9820.0,0.00\,F,F) S*ptKOSe_TV
Texts23B-3 TLX#39291rl File T»xt:VRXASQLE LABS
lOOSt A1.0SS8
eo:
so:
40:
20:
O.OEO
Tims
.4.3B5
.3.5S5
.2.SES
.1.7X5
.8.7E4
.O.OEO
Time
-2.3E7
^1.9E7
-1.4E7
.9 . 3E6
4.7E6
ISiOO 17:00 18:00 ISiOO 20-00 21:00
Pil«:X96423B #1-784 Acg: l-NOV-1996 20:41:16 OC SX+ Voltage SIR AutoSpae Stoise-5S4
317.9389 BSm{256,30,-3.0) PIO}{5,3,1,Q. 10*,2376. 0,0,00*,F,F) S*psZCOSF_TT
rnie Text:23B-3 TLI#39291rl Film Text:TRIANGLE LABS
2003! Al. E8
so:
eo:
40:
20:
22100
16tOO 17:00 ISiOO 19iOO 20iOO 21:00
P±le:I964238 #1-784 Acqt l-NOV-1996 20:41:16 OC EI+ Voltage SIR AutoSpec
375.8364 SxptZCONF_f7
Sample Text:233-3 TLI#39291rl Film Text,TRIANGLE LABS
22:00
O.OEO
Time
2.4S7
1.8E7
1.2E7
5.9E6
.0. OEO
Time
IftOO
17,00
233
-------
FiI»!XSS4S38 ii-734 Aogj t-iKV-i99e 2fl:4Ii« Off JET* Voltmgm SIR AuboSpmc SoiamtSiS
319.8965 BSVB(2S6,30, -3.0} PSS(S,3,l,0.10\,207S.O,O.QO>t,FtF) SxpsXCQ8P_TT
Sample Toxt:23B-3 TLI#39291rl Film Text: TRIANGLE LABS
801
601
401
201
0'
Film
321.
Soap
2003
ao:
so:
401
201
Film
327.
Sony)
1003
so:
601
401
201
0'
File
331.
San$>
1005
80:
601
401
20_
0
Filo
333.
Saatf
100S
80.
60-
40.
20.
0
fl
"'
l\ 1
65B6
i
I
\ AS.78S5
A AS.72B4 A7.51JB4
17:00 isl'00 15.-00 20:00 21s 00
1X964238 #1-784 Acg: l-NOV-1996 20i41sl6 OC SI* Voltage SIR AutoSpmc 8aismi2130
8936 BSUB(2S6,30, -3.0} PKD(5,3,1, 0.10%, 8520.0, 0. 00\,F,F) ExpsXCOSF TT
1m TmXt:23B-3 TLI#39291rl Film ToxtsTRIJOrQLS LABS
A4.07E6
"
Jl j
iT
1 AS, 2425 A3
S4SS
\ r*V\ . -A«A- A- - ,— —J^- -» *-* ^^J* A-~_
17:00 IflioO 15:00 20:00 21:00
SX964238 ^1-784 Aeqs l-SOV-1996 20:42:16 OC £T* Voltuym SIR AutoSpmc Noiee:499
8847 BSUB(2S6,30,-3.Q} PKD(5,3,1, 0.10%, 2SS6. 0, 0. 00%,F,FJ ExpiXCO8F_TT
1» Tmxti23B-3 TLI#39291rl Film Text : TRIAKOLE LABS
Al . Q8E8
11
'27:00 lai-oo is-00' ' ' ' '20-00' . ' ' '22-00
1X964238 #1-784 Acg: 1-SOV-1S96 20i41il6 OC KT+ Voltmff* SIR AutoSpac Noiemi636
9368 BSm(2S6,30,~3.0) PXD(5,3, 1, 0.10%, 2544. 0, 0. 00*,P,F) ExpiXCONF TT
1m Tmxti23B-3 Til#35251rl Film Toxt t TRIANOLS LABS
A7.29S7
h
,
III
I
I
' 17:00 18:00 25:00 20-00' ' ' ' '2li00'
tI964238 #2-784 Acg: 1-IK1V-1996 20i41sl6 QC EI+ Voltage SIR AutoSpmc Noise: 53 4
9338 BSm{256,30,-3.0) PXDtS,3,l,0.10X,2136.Q,O.Oa*,F,F) SxpiXCONF_TT
1m Text:23B-3 TLI#39291rl Film Text : TXIJUraLS LABS
J&.1SS7
A
27:00
r
ID
18:00 25:00
1
ft
20:00 . 21-00
_S,2S5
_3.SES
_2.«B5
" 0.QBO
Time
_8.32S
,e.7ES
-5. OES
_3 . 3ES
_1.7E5
Time
.1 . 7E7
'.1.3E7
.8.5E6
'-4.2E6
" 0. OEO
Time
-1.4E7
'.1.2E7
.8.7E6
.S.8E6
.2.9E6
O.OEO
Timm
-1.8E7
.1.4E7
-2.1S7
-7.1B6
-3.5S6
.O.QSO
Time
3 JO
-------
?il*:XS64238 #1-784 Aagt 1-IKJV-19S6 20t41il6 OC SI* Volt»ff» SIS AvtoSpme
303.9016 ExfsXCOSF_TT
Saapla fmxtt23B-3 TLI#39291rl Film Text : TRIAtraLE LABS
IOCS
80:
~
601
401
201
o-
18 113 18,43
17:31 1
16«24 1 I \
20.32
n AW/iTfi MA n "i'Ti T2Tsr .
/ \ 16:54 " U \ f V y\ II f\/l/\«\ IV
J ^uu«u v U Hu w w v yu LJ y
r 1 1 1 1 1 ' 1 ' ' ' I T I I 1 ' r ] 1 i -i i i ]~ i -r
16sOO 17:00 18:00 15*00 20:00
1 A A/L:04 '22'"2*
.3.7S5
.3. DBS
-2.2K5
.2 . 5«5
-7.4F4
O.OBO
J2J. 2 00 2J? * 00 7xm0
FiiasX964238 #1-784 Acgs 1-1KJV-15S6 20.'4isl6 OC SI* Voltage SIR AutoSpmc
315.9419 SxpiXCQSF_TT
S«ss5le fwre:23B-3 FI,X#3S2Slrl Film fmxtsTRIAllQLS MBS
1003
80:
601
401
201
o-
20
J
16-00 17-00 18:00 15:00 20:00
:22
I
-2.3S7
.1.5B7
.1.4X7
-9.3S6
_4 . 7SS
O.OBO
21:00 -22 1-00 I-lae
F±le:X964238 #1-784 Aaqs 1-NOV-199S 20:41:16 OC ET* Voltage SIR AutoSpmc
315.8565 SxpsXCONF_TT
Sans>l8 J"«rt:23B~3 FLI#39291rl Film Tmxt:TRIANQZ*S LABS
iooa
so:
60:
40:
20:
0'
17 02
i 17:33
t i
1
f\ 18:32
\ \ 18:11 j " 15:27
. ^__J \ / L_J^AW\^Av_>f^>/«v«^*WV^^**l'^
•^ n ""^ -» r-"~ -•-* -\j
-6. 6S7
.S.3B7
.4 . OS7
'.2.6E7
11.3X7
' O.OEO
SliQQ ' ' ' '22tOO ' ' ?la»
3-n
-------
Peak Locate Examination: l-NOV-1996:20:40 File:X964238
Experiment:XCONF_TT Function:1 Reference:PFK
Volts
0.6117
292.95315
292.98245
293.01175
Volts
0.6136
330.94615
330.97925
331.01235
-------
TLI Project: 39291rl
Client Sample: 23FB-4
Method 23 PCDD/PCDF Analysis (a)
Analysis File: T966607
Client Project:
Sample Matrix:
TLI ID:
Sample Size:
Dry Weight:
GC Column:
Eastern Ridge Lime Facility
M23TRAIN
143-23-7A,B
1.000
n/a
DB-5
Date Received:
Date Extracted:
Date Analyzed:
Dilution Factor:
Blank File:
Analyst:
10/19/96
10/21/96
11/01/96
n/a
T966616
B6
Spike File:
ICal:
ConCal:
% Moisture:
% Lipid:
% Solids:
SPX23704
TF53286
T966598
n/a
n/a
n/a
2,3J,8-TCDD
1,2,3,7,8-PeCDD
1,2,3,4,7,8-HxCDD
1,2,3,6,7,8-HxCDD
1,2,3,7,8,9-HxCDD
1,2,3,4,6,7,8-HpCDD
1,2,3,4,6,7,8,9-OCDD
2,3,7,8-TCDF
1,2,3,7,8-PeCDF
2,3,4,7,8-PeCDF
1,2,3,4,7,8-HxCDF
1,2,3,6,7,8-HxCDF
2,3,4,6,7,8-HxCDF
1,2,3,7,8,9-HxCDF
1,2,3,4,6,7,8-HpCDF
1,2,3,4,7,8,9-HpCDF
1,2,3,4,6,7,8,9-OCDF
'•••'^X+£-^<<-sX^
Total TCDD
Total PeCDD
Total HxCDD
Total HpCDD
Total TCDF
Total PeCDF
Total HxCDF
Total HpCDF
M
ND
ND
ND
ND
ND
0.01
0.18
ND
ND
ND
ND
ND
0.006
ND
0.006
ND
0.02
ND
ND
ND
0.01
ND
ND
0.006
0.006
0.005
0.008
0.01
0.01
0.009
1.18 29:15
0.83 31:43
0.005
0.005
0.005
0.007
0.006
1.11 25:55 B_
0.008
1.01 28:19
0.01
0.85 31:46
0.005
0.008
0.01
1
0.005
0.005
1 •
1
Page 1 Of 2 X257 J>SR vl.14. LARS 6X8.00
Triangle Laboratories, Inc.®
801 Capftola Drive * Durham, North Carolina 27713
Phone: (919) 544-5729 « Fax: (919) 544-5491
Printed: 16:05 11/11/96
•1 •
'
-------
TLI Project: 39291rl
Client Sample: 23FB-4
Method 23 PCDD/PCDF Analysis (a)
Analysis File: T966607
l3C12-2,3,7»8-TCDF
>3C12-2,3,7,8-TCDD
13C,2-l,2,3,7,8-PeGDF
13C,2-l,2,3,7,8-PeCDD
13C12-l,2,3»6,7,8-HxCDF
»C,2-l,2,3,6,7,8-HxCDD
13C,2-l,2,3,4,6,7,8-HpCDF
13C,2-l,2,3,4,6,7»8-HpCDD
13e12-l,2,3,4,6J,8,9-OCDD
3.2
3.5
3.1
2.9
3.8
4.0
3.9
3.8
5.7
81.2
86.5
77.7
72.2
95.1
99.5
96.3
94.8
71.4
40%-130%
40%-130%
40%-130%
40%-130%
40%-130%
40%-130%
25%-130%
25%-130%
25%-130%
0.76
0.79
1.52
1.49
0.49
1.25
0.43
1.06
0.83
15:36
16:22
20:51
22:18
25:20
26:10
28:18
29:14
31:42
37CLr2,3,7,8-TCDD
»C,2-2,3(4,7,8-PeCDF
13C,2-U,3,4,7,8-HxCDF
13Cl2-l,2,3,4,7,8-HxCDD
13Ci2-l,2,3,4,7»8,9-HpCDF
3.9
3.7
4.1
3.9
3.8
96.3
93,0
103
97.3
95.8
70%-140%
70%-140%
70%-140%
70%-140%
70%-140%
1.50
0.49
1.23
0.42
16:24
21:50
25:13
26:05
29:33
13Ci2-l,2,3,7,8,9-HxCDF
'3Ci2-2,3,4,6,7,8-HxCDF
4.1
3.7
104
93.5
40%-130%
40%-130%
0.48
0.49
26:40
25:55
13Ci2-l,2,3,4-TCDD
l3C,2-l,2,3»7,8,9-HxCDD
0.80
1.22
16:09
26:29
Data Reviewer.
11/11/96
Page 2 of2
XS7J>Sl»I.I4tLARS««.!»
Triangle Laboratories, Inc.®
801 Capitola Drive • Durham, North Carolina 27713
Phone: (919) 544-5729 * Fax: (919) 544-5491
Printed: 16:05 11/11/96
3" 4
-------
TLI Project: 39291rl
Client Sample: 23FB-4
Toxicity Equivalents Report
Analysis File: T966607
Client Project:
Sample Matrix:
TLI ID:
Sample Size:
Dry Weight:
GC Column:
Eastern Ridge Lime Facility
M23TRAIN Date Received: 10/19/96
143-23-7A,B Date Extracted: 10/21/96
Date Analyzed: 11/01/96
1.000 Dilution Factor: n/a
n/a Blank File: T966616
DB-5 Analyst: BB
Spike File:
ICal:
ConCal:
% Moisture:
% Lipid:
% Solids:
SPX23704
TF53286
T966598
n/a
n/a
n/a
Anafytes
2,3,7,8-TCDD
1,2,3,7,8-PeCDD
1,2,3,4,7,8-HxCDD
1,2,3,6,7,8-HxCDD
1,2,3,7,8,9-HxCDD
1,2,3,4,6,7,8-HpCDD
1,2,3,4,6,7,8,9-OCDD
TOTAL PCDD
2,3,7,8-TCDF
1,2,3,7,8-PeCDF
2,3,4,7,8-PeCDF
1,2,3,4,7,8-HxCDF
1,2,3,6,7,8-HxCDF
2,3,4,6,7,8-HxCDF
1,2,3,7,8,9-HxCDF
1,2,3,4,6,7,8-HpCDF
1,2,3,4,7,8,9-HpCDF
1,2,3,4,6,7,8,9-OCDF
TOTAL PCDF
Amt.(ng)
0.005
0.008
0.01
0.01
0.009
0.01
0.18
0.005
0.005
0.005
0.007
0.006
0.006
0.008
0.006
0.01
0.02
Total
X
X
X
X
X
X
X
X
X
X
X
X
X
X
X
X
X
EPA TEFs,
t££
1
0.5
0.1
0.1
0.1
0.01
0.001
0.1
0.05
0.5
0.1
0.1
0.1
0.1
0.01
0.01
0.001
1989a: 0.0183 ng
Equivalent
0.005
0.004
0.001
0.001
0.0009
0.0001
0.00018
0.0122
0.0005
0.00025
0.0025
0.0007
0.0006
0.0006
0.0008
0.00006
0.0001
0.00002
0.00613
Page 1 of 1
TEFPR v5.08, LARS 6.08.00
Triangle Laboratories, Inc.®
801 Capitola Drive • Durham, North Carolina 27713
Phone: (919) 544-5729 • Fax: (919) 544-5491
Printed: 16:22 11/11/96
-------
Data Review By:
..Date.
Calculated Noise Area:
2.49
The Total Area £or each peak with an ion abundance ratio outside
ratio limits has been recalculated according to method requirements.
Page No.
11/11/96
Listing of T9666Q7B.dbf
Matched GC Peaks / Ratio / Ret. Time
Compound/
M_Z.... QC.Log omit Why ..RT. OK Ratio Total.Area... Area.Peak.1.. Area. Peak. 2. . Rel.RT Compound. Name-.. ID.
TCDP
304-306
304-306
13C12-TCDF
316-318
316-318
TCDD
320-322
DC
DC
DC
DC
DC
DC
DC
DC
DC
DC
DC
DC
DC
DC
DC
DC
DC
DC
DC
DC
DC
DC
DC
DC
DC
DC
DC
DC
DC
DC
DC
NL
SN
SN
SN
SN
SN
SN
SN
SN
SN
SN
SN
SN
SN
SN
SN
SN
SN
SN
SN
WH
WH
WH
0
NL
WH
4
NL
SN
SN
SN
SN
SN
0
13
13
14
14
14
14
14
15
IS
15
15
15
15
16
17
17
17
17
17
17
17
18
:00
:48
:53
:09
:24
:28
:41
:45
:01
:12
:17
:37
:53
:59
:S9
:08
:11
:18
:38
:42
:SO
.57
:02
0
RO
RO
RO
RO
RO
RO
RO
RO
RO
RO
RO
RO
RO
RO
RO
RO
RO
RO
RO
.65-0.89
1
0
1
0
0
0
1
0
0
0
1
0
0
1
0
0
0
0
0
0
0
0
0
.03
.46
.04
.17
.89
.22
.92
.91
.34
.91
.04
.99
.42
.14
.58
.80
.82
.53
.22
.88
.42
.28
.31
Peaks
0
14
15
15
16
17
:00
= 38
:11
:36
:03
:35
0
RO
RO
RO
RO
1
0
0
0
2
0
0
0
0
2
1
3
0
0
0
0
0
2
•1
0
0
0
0
0
.26
.99
.80
.27
.31
.32
.67
.80
.69
.50
.48
.61
.63
.39
.48
.79
.40
.56
.07
.77
.51
.26
.58
.00
.65-0.89
1
0
0
0
1
0
Peaks
0
13
14
14
14
:00
:S3
:05
:27
:38
14:46
0
RO
RO
RO
RO
RO
RO
.17
.84
.56
.76 4,
.01
.52
4,
2
53
11
835
42
5
942
r*v">rv
,65-0.89
17
5
3
1
7
0
.00
.78
.32
.50
.89
.91
0
0
0
0
0
0
.36
.66 24.52
.25 4.90
.43 2,080.72
.04 24.01
.78
.38
.05
.16
.34
.50
.16
.62
0.828-1.138
0
0
0
0
0
0
0
0
0
0
0
1
1
1
1
1
1
1
1
1
1
1
1
.000
.885
.890
.907
.923
.927
.941
.946
.963
.974
.980
.001 2378-TCDF AN
.018
.025
.089
.098
.101
.109
.130
.135
.143
.151
.156
0.936-1.064
0
29.14 0
8.73 0
2,754.71 1
23.73 1
1
.000
.938
.973
.000 13C12-2378-TCDF ISO
.029
.127
0.846-1.086
0
0
0
0
0
0
.000
.848
.860
.883
.894
.902
Triangle Laboratories, Inc.® Analytical Services Division
801 Captota Drive • Durham, North Carolina 27713
Phone: (919) 544-5729 • Fax: (919) 544-5491
Printed: 15:5411/11/96
3 6
-------
Page No.
11/11/96
Listing of T9666Q7B.db£
Matched GC Peaks / Ratio / Ret. Time
Compound/
M_Z.... QC.Log Omit why ..RT. OK Ratio Total.Area... Area.Peak,1,. Area.Peak.2.. Rel.RT compound.Name., ID.
0.905
0.913
0.923
0.939
0.945
0.954
0.963
0.981
0.988
0.995
1.002 2378-TCDD AN
1.011
1.030
1.041
1.053
1.059
1.063
1.079
320-322
37C1-TCDD
328
328
13C12-TCDD
332-334
332-334
PeCDF
340-342
DC
DC
DC
DC
DC
DC
DC
DC
DC
DC
DC
DC
DC
DC
DC
DC
DC
DC
DC
DC
SH
SN
SH
SN
SN
SN
SN
SN
SS
SN
SN
SN
SN
SN
SN
SN
SN
SN
WH
0
NL
14:
14:
15:
15:
15:
15:
15:
16:
16:
16:
16:
49
57
06
22
28
37
46
03
10
17
24
RO
RO
RO
RO
RO
RO
RO
RO
16:33
16:51
17:02
17:14
RO
RO
17:20
17:24
17:40
17 ;
i53
RO
RO
0.
0.
0.
0.
1.
1.
0.
0.
3.
0.
0.
0.
0.
1.
4.
0.
0.
0.
1.
41
79
72
63
57
71
46
72
83
35
35
70
84
35
78
81
78
23
07
Peaks
0:
tOO
14:57
16:24
DC
DC
SN '
2
NL
16,
:40
Peaks
0:00
15:09
16
:09
0.
RO
RO
3,
3,
0.
0.
1.
1.
0.
2.
0.
0,
1.
1,
2.
2.
1.
0.
0.
0.
1.
0.
0.
0.
0.
24.
839.
1.
863.
43
70
65
36
90
37
80
91
68
14
81
92
47
92
16
94
55
61
53
00
.02
.38
,57
,43
,95
65-0.89
2
1
.38
.00
0.80 4,
16:22
16:47
DC
DC
DC
DC
DC
DC
DC
DC
DC
DC
DC
DC
DC
4
NL
WL
SN
SN
SN
SN
SN
SN
SN
SN
SN
SN
SN
0
0
Peaks
0
17
17
17
18
18
18
:00
:47
:54
:58
:01
:11
:15
18:40
18
19
19
19
19
:56
:08
:14
:29
:53
1.
RO
RO
RO
RO
RO
RO
RO
RO
RO
RO
RO
RO
.79 4,
.71
9,
4.
13.
705,
268
45
033
FTWTHI
.11
.51
.77
.37
.72
.37
"l /
32-1.78
0
0
0
0
1
0
0
0
0
0
0
1
2
.11
.72
.34
.92
.02
.35
.42
.88
.51
.43
.07
.36
.68
0
0
0
0
2
0
1
1
0
0
0
1
2
.07
.97
.26
.95
.12
.43
.16
.87
.54
.69
.05
.06
.22
24.38
3,839.57
7.64
2,093.79
1,881.68
19.04
Follows
1.093
0.878-1.122
0.000
0.913
1.002 37C1-TCDD SUR1
1.018
0.878-1.122
0.000
7.63 0.926
2,611.98 0.987 13C12-1234-TCDD RSI
2,386.69 1.000 13C12-2378-TCDD IS1
26.68 1.025
.855-1.112
0.000
0.853
0.859
0.862
0.864
0.872
0.875
0.895
0.908
0.918
0.922
0.934
0.954
Triangle Laboratories, Inc.® Analytical Services Division
801 Capitola Drive • Durham, North Carolina 27713
Phone: (919) 544-5729 • Fax: (919) 544-5491
Printed: 15:5411/11/96
37
-------
Page No.
11/11/96
Listing of T966607B.dbf
Matched GC Peaks / Ratio / Ret. Time
Compound/
M_Z.... QC.Log Omit Why ..RT. OK Ratio Total.Area Area.Peak.1.. Area.Peak.2.
Rel.RT Compound.Name.. ID.
340-342
13C12-PeCDF
352-354
352-354
PeCDD
356-358
DC
DC
DC
DC
DC
DC
DC
DC
DC
DC
DC
DC
DC
DC
DC
DC
DC
DC
DC
DC
DC
DC
DC
DC
DC
DC
DC
DC
DC
DC
DC
DC
DC
DC
DC
DC
DC
DC
SN
SN
SN
SN
SN
SN
SN
SN
SN
SN
SN
SN
SN
SN
SN
SN
SN
SN
SN
SN
SN
WH
WH
WH
0
NL
SN
SN
SN
6
NL
SN
SN
SN
SN
SN
SN
SN
SN
SN
20
20
20
20
20
20
20
20
21
21
21
21
21
21
22
22
22
22
22
23
23
23
23
23
:05
:12
:17
:23
:27
:32
:47
:53
:00
:15
:29
:40
:44
-.52
:01
:09
:14
:35
:56
:03
:07
:17
:23
:27
RO
RO
RO
RO
RO
RO
RO
RO
RO
RO
RO
RO
RO
RO
RO
RO
RO
RO
RO
RO
RO
1
0
1
2
1
0
1
0
0
0
0
0
0
2
1
2
0
0
1
0
0
0
0
3
.50
.34
.08
.86
.29
.57
.48
.65
.22
.30
.27
.28
.67
,82
.23
.85
.93
.67
.57
.63
.53
.25
.41
.00
Peaks
0
19
20
20
21
21
21
22
22
23
:00
:39
:24
:51
:04
:15
:50
:1S
-.19
:00
1.
RO
RO
RO
RO
RO
RO
32
0
1
2
1
1
1
1
2
1
0
Peaks
0
19
19
20
20
20
20
20
20
20
:00
-.47
:57
:02
:16
:20
:33
:39
:45
:58
1.
RO
RO
RO
RO
RO
RO
RO
RO
RO
RO
-1.78
.75
.29
.07
,52
.20
.64
.50
.60
.47
.90
.32-1.78
10
0
0
0
0
1
2
2
2
0
.50
.96
.31
.57
.62
.21
.52
.27
.90
.43
0
0
0
0
0
0
1
1
0
0
0
0
0
0
0
0
0
1
2
0
0
0
0
0
0
.85
.53
.44
.54
.95
.95
.39
.18
.32
.53
.51
.35
.33
.97
.71
.51
.41
.04
.83
.17
.74
.60
.61
.54
.00
0
0
0
0
0
0
0
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
.963
.969
.973
.978
.981
.985
.997
.002 12378-PeCDF AN
.007
.019
.030
.039
.042
.049 23478-PeCDF AN
.056
.062
.066
.083
.100
.106
.109
.117
.122
.125
0.808-1.192
0
40
15
4,414
23
28
4,176
1
5
4
.05
.15 24.39
.56 12.62
.20 2,661.94
.96 14.58
.57 17.74
.94 2,508,40
.61
.72
.18
0
18.93 0
6.11 0
1,752.26 1
12.12 1
10.83 1
1,668.54 1
1
1
1
.000
.942
.978
.000 13C12-PeCDF 123 IS2
.010
.019
.047 13C12-PeCDF 234 SUR2
.067
.070
.103
8,699,38
: P©CX)F / P0CDD F O I X ows — —
0
1
0
0
1
1
1
0
0
0
-OS
.28
.94
.86
.22
.25
.12
.56
.26
.54
0.885-1.034
0
0
0
0
0
0
0
0
0
0
.000
.887
.895
,898
.909
,912
,922
.926
.930
.940
Triangle Laboratories, Inc.® Analytical Services Division
801 Captola Drive • Durham, North Carolina 27713
Phone: (919) 544-5729 • Fax: (919) 544-5491
Printed: 15:5411/11/96
3--/S
-------
Page No.
11/11/96
Listing of T9666Q7B.dbf
Matched GC Peaks / Ratio / Rat. Time
Compound/
M_Z..., QC.Log Omit Why ..RT. OK Ratio Total.Area... Area.Peak.1.. Area.Peak.2.. Rel.RT Compound.Kama., ID.
356-358
13C12-PeCDD
368-370
368-370
HXCDF
374-376
WK
374-376
DC
DC
DC
DC
DC
DC
DC
DC
DC
DC
DC
DC
DC
DC
DC
DC
DC
DC
DC
DC
DC
DC
DC
DC
DC
DC
DC
DC
DC
DC
DC
DC
DC
DC
DC
DC
DC
DC
SN
SN
SN
SN
SN
SN
SN
SN
SN
WH
WH
WH
0
NL
SN
SN
2
NL
SN
SN
SN
SN
SN
SN
SN
SN
SN
SN
SN
SN
SN
SN
SN
SN
SN
SN
SN
WH
WH
WH
1
21:
21:
21:
21:
22:
22:
22:
22:
22:
23:
23:
23:
08
25
34
42
10
20
36
50
57
05
11
16
RO
RO
RO
RO
RO
RO
RO
RO
RO
RO
RO
2.
1,
0.
2.
0.
2.
2.
0.
1.
0.
4.
2.
54
68
98
59
51
73
19
83
21
93
33
12
Peaks
0:
21:
22:
22:
22:
00
07
18
28
53
1.
RO
RO
RO
1.
0.
0.
0.
0.
1.
0.
1.
1.
0.
0.
1.
0.
22
75
82
56
64
50
66
OS
55
69
54
05
00
32-1.78
1.
1.
1.
1.
1.
Peaks
0:00
1.
RO
23:57
24:08
24:11
24:15
24:18
24;
:30
24:35
24:38
RO
RO
RO
RO
RO
RO
RO
24:44
25:06
25:10
25
25
25
26
26
26
26
26
26
27
27
27
:40
:48
:55
:00
:31
:32
:36
:44
:46
:02
:06
:11
RO
RO
RO
RO
RO
RO
RO
RO
RO
RO
00
91
49
51
13
0.
1.
2,407.
242.
5.
2,649.
•n~.f*ft*tf-
05-1.43
2.
1.
0,
,63
,33
,76
0.50
0.42
4.
,43
6.50
0.63
2,
1,
1
1
0
0
1
1
,0
1
2
0
0
1
1
0
.24
.22
.09
.06
.44
.71
.11
.67
.77
.24
.53
.45
.81
.51
.71
.30
Peak
0.
0.
0,
05
43
97 1,439.37
00 145.50
41
97
/fS-ff^TVtf I-?***! 1 t~ft f e ~.
,78
,63
,61
0.14
0.33
0.63
0.09
0.31
0.56
0,
.60
0.67
0
0
0
5
0
0
0
0
0
0
1
0
0
5
.68
.22
.70
.41 2.85
.20
.83
.47
.85
.83
.78
.10
.31
.43
.41
0.
0.
0.
0.
0.
1.
1.
1.
1.
1.
1.
1.
948
960
967
973
994
001 12378-PeCDD
013
024
029
035
040
043
0.821-1.179
0.
0.
968.60 1.
000
947
000 13C12-PeCDD 123
96.50 1.007
1.026
0.945-1.064
0.000
0.945
0.
.953
0.955
0.957
0.959
0.967
0.970
0.972
0.976
0.991
0.993
1
1
2.56 1
1
1
1
1
1
1
1
1
1
.013
.018
.023 234678-HxCBF
.026
.047
.047
.050
.055 123789-HXCBF
.057
.067
.070
.073
1S3
Triangle Laboratories, Inc.® Analytical Services Division
801 Caprtote Drive • Durham, North Carolina 27713
Phone: (919) 544-5729 • Fax: (919) 544-5491
Printed: 15:54 11/11/96
3 9
-------
Page No.
11/11/96
Listing of T966607B,dbf
Hatched GC Peaks / Satio / Set. Tims
Compound/
M_Z QC.Log Omit Why .,RT. OK Ratio Total.Area... Area.Peak.1.. Area.Peak.2.. Rel.RT Compound.Name.. ID..
13C12-HXCDF
384-386
384-386
HxCDD
390-392
390-392
13C12 -HxCDD
402-404
402-404
DC
DC
DC
DC
DC
DC
DC
DC
DC
DC
DC
DC
DC
DC
DC
DC
DC
DC
DC
DC
DC
DC
DC
DC
DC
NL
SN
SN
SN
SN
6
NL
WL
SN
SN
SN
SN
SN
SN
SN
SN
SN
SN
SN
SN
SN
SN
WH
0
NL
SN
SN
3
0:00
24:05
24:15
25:13
25:20
25:55
26:22
26:28
26:40
26:51
26:54
Peaks
0:00
24:32
24:37
24:44
24:50
24:50
25:13
25:21
25:26
25:39
25:43
25:52
26:03
26:25
26:28
26:32
26:43
PeaJcs
0:00
25:30
26:05
26:10
26:22
26:29
Peaks
0.
RO
RO
RO
RO
RO
1.
RO
RO
RO
RO
RO
RO
RO
RO
RO
RO
RO
RO
RO
RO
RO
1.
RO
RO
43-0.59
1.
0.
0.
0.
0.
0.
1.
0.
0.
1.
0.
39
52
52
49
49
49
17
66
48
38
69
1
20
20
3,161
3,286
3,066
0
I
2,766
3
3
12,321
05-1.43
0.
0.
0.
3.
0.
0.
5.
7.
0.
0.
0.
0.
0.
1.
2.
1.
2.
40
46
31
00
20
24
65
00
96
24
44
25
97
23
16
12
00
0
0
0
0
0
0
0
0
0
0
0
0
1
0
0
0
0
0
.50
.17
.25
.72
.05
.97
.98
.90
.71
.57
.47
.87
P I tlvd
t / tlX1
.61
.31
.27
.56
.07
.23
.52
.60
.40
.22
.44
.36
.21
.87
.69
.87
.40
.00
.05-1.43
1.
1.
1.
1.
0.
33
03
23
25
84
1.22
1
5
2,350
2,687
2
2,863
7,902
i • Mvrn
.07
.53
.78
.33
.96
.95
.06
in / My
0.842-1.158
0
6.94 13.23 0
6.93 13.32 0
1,039.28 2,122.44 0
1,086.26 2,199.79 1
1,001.88 2,065.09 1
1
1
895.09 1,871.62 1
1
1
F_T 1 j"\TJC ™. _ — _«_,__
0.939
0
0
0
0
0
0
0
0
0
0
0
0
0
1
1
1
1
0.962
0
0
1,298.82 1,051.96 0
1,492.17 1,195.16 1
1
1,574.06 1,289.89 1
.000
.951
.957
.995 13G12-HXCDF 478
.000 13C12-HXCDF 678
.023 13C12-HXCDF 234
.041
.045
.053 13C12-HXCDF 789
.060
.062
-1.017
.000
.938
.941
.945
.949
.949
.964
.969
.972
.980
.983
.989
.996
.010
.011 123789-HxCDD
.014
.021
-1.038'
,000
.975
.997 13C12 -HxCDD 478
.000 13C12 -HxCDD 678
.008
.012 13C12-HXCDD 789
SUR3
IS4
ALT2
ALT1
AN
SOR4
IS5
RS2
HpCDF
408-410
0.88-1.20
DC NL 0:00 1.03
28:19 1.01
DC SN 28:26 RO 3.71
DC SN 2S:34 RO 0.81
0.69
6.37
0.78
1.51
3.20
0.995-1.051
0.000
3.17 1.001 1234678-HpCDF
1.005
1.009
AN
Triangle Laboratories, Inc.® Analytical Services Division
801 Capitals Drive • Durham, North Carolina 27713
Phone: (919) 544-5729 • Fax: (919) 544-5491
Printed: 15:54 11/11/96
310
-------
Page No.
11/11/96
Listing of T966607B.dbf
Matched GC Peaks / Ratio / Ret. Time
Compound/
M_Z.... QC.Log Omit Why ..RT. OK Ratio Total.area... Area.Peak.1.. Area,Peak.2.. Rel.RT Compound,Name.. ID.
408-410
13C12-HpCDF
418-420
418-420
HpCDD
424-426
MK
424-426
13C12-HpCDD
436-438
436-438
OCDF
442-444
442-444
DC
DC
DC
DC
DC
DC
DC
DC
DC
DC
DC
DC
DC
DC
DC
DC
DC
DC
DC
DC
DC
DC
DC
DC
DC
DC
DC
SN
SN
SN
SN
SN
WH
WH
1
NL
2
NL
SN
SN
SN
SN
SN
SN
SN
WH
WH
WH
1
NL
2
NL
SN
SN
SN
SN
SN
SN
1
28
•28
29
:40
:55
:03
29:07
29
29
:42
:57
30:01
RO
RO
RO
RO
RO
RO
1.
0.
0.
2.
0.
0.
0.
25
88
06
52
14
56
30
Peak
0
28
29
:00
:18
:33
0.
RO
1.
0.
0.
0.
0.
0.
0.
6.
94
81
08
43
36
79
31
37
37-0.51
1.
0.
0.
Peaks
0
28
28
28
28
28
29
29
29
-29
29
29
;00
:30
:36
:46
:52
:58
:02
:1S
:24
s32
:42
:45
0.
RO
RO
RO
RO
RO
RO
RO
RO
RO
14
43
42
1.
2,265.
1,712.
3,977 .
88-1.20
0.
1.
0.
1.
4.
0.
0.
1.
1.
2.
0.
0.
03
03
94
69
so
85
69
18
26
23
67
48
Peak
0
-28
29
:00
:36
= 14
0.
RO
0.
0.
3.
1.
0.
1.
0.
5.
0.
1.
0.
0.
5.
90
04 677.33
15 508.11
19
02
75
87
10
20
12
88
25 2.84
47
77
24
43
25
88-1.20
0.
0.
1.
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0
28
29
29
29
29
31
32
:00
:53
:13
:22
:44
:50
:46
5 16
0.
RO
95
87
06
*\» A. ..*.
76-1.02
1.13
1.
6.
2,090.
29
74 3.43
22 1,075,63
2,096.96
: HpCDD / Octa— CDD and CDF
0.
0.86 1.
RO
RO
RO
RO
1.
,11
1.90
0.74
1.
.18
0.85
RO
1.
.06
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0,
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,49
.34
0.91
1.15
1.27
8.93 4.10
0,
.64
1.
1.
1.
1.
1.
1.
1.
013
022
027
029
049
058
061
0.929-1.141
0.
1,587.71 1.
1,204.04 1.
000
000 13C12-HpCDF 678
044 13C12-HpCDF 789
IS6
SUR5
0.973-1.006
0.000
0.
975
0.978
0.984
0.987
0.
,991
0.993
2.41 1.001 1234678-HpCDD
AN
1.006
1.010
1.
1,
.016
,018
0.966-1.034
0
3.96 0.
1,014.59 1
.000
.978
.000 13C12 -HpCDD 678
IS7
0.874-1.126
0
0
0
0
0
0
4.83 1
1
.000
.911
.922
.926
.938
.941
.002 OCDF
.018
AN
8.93
Triangle Laboratories, Inc.® Analytical Services Division
801 Capitola Drive « Durham, North Carolina 27713
Phone: (919) 544-5729 • Fax: (919) 544-5491
Printed: 15:5411/11/96
311
-------
Page No.
11/11/96
Listing of T96660"7B.dtof
Matched GC Peaks / Ratio / Ret. Time
Compound/
M_Z.... QC.Log Omit Why .,RT. OK Ratio Total.Area... Area.Peak.1.. Area.Peak.2.. Rel.RT Compound,Hame.. 10.
OCDD
458-460
458-460
0.76-1.02
DC NL 0:00 RO 1.50
DC SN 31:33 RO 1.26
31:43 0.83
DC SN 32:03 RO 1.91
1 Peak
0.04
0.79
55.76
0.87
55.76
25.27
0.874-1.126
0.000
0.995
30.49 1.001 OCDD
1.011
AH
13C12-OCDD 0.76-1.02
470-472 DC ML 0:00 1.00 0.04
31:42 0.83 2,463.54
470-472 1 Peak 2,463.54
1,120.76
0.995-1.006
0.000
1,342.78 1.000 13C12-OCDD
IS8
Column Description. "Why Code Description QC Log Desc,
M_2 -Nominal Ion Mass{es)
. .RT. -Retention Time {ram-.ss)
Rat.l -Ratio of M/M+2 Ions
OK -RO=Ratio Outside Limits
Ral.RT-Relative Retention Time
End of Report
WL-Below Retention Time Window
WH-Above Retention Time Window
SN-Below Signal to Noise Level
-------
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801
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201
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10 04 AS.69E6
801
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40.
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02:17
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20:00 21:00 22:00
Fils:T966607 #1-835 Acqsl-NOV-96 02:14:12 EI+ Voltage SIX 70T
330.9792 F:2 ExpsEPCUS
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23:00
100*
801
601
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201
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-------
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TRIANGLE LASS Texti23FB-4 TLI#39291X1 HKT. TIME - 02:17
100S A3, 2E3
24:36 24s48 25:00 25:12 25:24 25:36 25:48 26:00 26:12 26:24 26:36 26:48
F±le:T966607 #1-505 Acq:l-IfOV-96 02:14:12 EH- Voltaye SIB 70T NoiaesSOS
401.8558 Fs3 BSDS(256,30, -3. 0) JPJOJfS,3,1, 0.101,1220. 0,0. 001,F,F) Exp:EPCUS
TRIANGLE LASS Text:23FB-4 TLH39291S1 IJVJ. TIMS = 02:17
lOOSt A1.57E7
A1.49E7
801
60.
40,
20.
24:36 24:48 25:00 25:12 25:24 25:36 25:48 26:00 26';12 26:24
File:T966607 #1-505 Acqsl-mV-96 02:14:12 EI+ Voltage SIR 7QT Koines232
403.8529 F:3 BSDS(256, 30,-3 .0) PKD(5,3,1, 0.101,928. 0, 0.00*,F,F) Exp:EPCUS
TRIANGLE LABS Text:23FB~4 TZIt39291Xl JKT. TIME - 02:17
A1.29E7
A1.20E7
801
60.
40.
26:36 26:48
24s36 24:48 25:00 25:12 25:24 25:36 25:48 26:00 26:12
File:T966607 fl-505 Acq:l-NOV-96 02:14:12 EI+ Voltage SIS 70T
392.9760 f:3 SxpsSPCUB
TRIANGLE LABS Texti23FB~4 TLH39291R1 JK7. TIME
Iooat 24:4824:57 25:1125^20 25:47 26:03
401
201
0,
26:24 26:36 26:48
02:17
26:34 26:44
O.OEO
Time
24:36 24:48 25:00 25:12 25:24 25:36 25:48 ' 'sCtOQ ' 26.-12 ' '26:24 ' ^26t36 ' 26:48
.5.0E6
.4.0E6
.3. OE6
.2.0E6
.1. OE6
.O.OEO
Time
.4.2E6
.3.3E6
.2.5E6
.1. 7E6
.8.3E5
.O.OEO
Time
.6.0E6
.4.8E6
.3. 6E6
.2.4E6
.1.2S6
.O.OEO
Time
313
-------
FiletT966607 #1-443 Acq:l-NOV-96 02:14:12 EH- Voltage SIS 70T Noise: 176
407.7818 F:4 BSUB(256,30, -3. 0) PKD(5,3,1, 0.10%, 704.0, 0. 00*,F,F) Exp:EPCUS
TRIANGLE LABS Text:23FS-4 TLI#39291S1 IMT, TIME "
lOOt
so:
60:
40:
20:
A3 . 20E4
fA A1.41E4
^} vx /\ JYJ-_^J~ ,,-js - ••»
28:12 28:24 28:35 28:48
File:T966607 #1-443 Acq ; 1 -1KJV-96 02:14:12
409.7789 F:4 BSUS(256,30,-3.0) PKD(5,3,1,0
TRIANGLE LABS Text:23FB-4 TOT #3 9291X1
1001
80:
60:
40:
201
o"
A3.17E4
JH A ^4.35£3 A9.50E3
28:12 28-24 28:35 28:48
File sT9 6 66 07 #1-443 Acqsl-NOV-96 02:14:12
417.8253 F:4 BSUB(256,30,-3.0) PKD(5, 3,1,0
TRIANGLE LABS Text:23FS-4 TLI939291S1
1003
so:
so:
40:
20:
o-
A6 . 77E6
l\
\
28:12 2B\2t 26136 3B;itt
29:00
29:12 ' ' ' 29:24 '
ZI+ Voltaye SIK 70T Noises 171
,10%,684.0,0.00%,F,F,> acpzEPCPS
JKJ. TIME «
02:17
29836'
02:17
_8.4Jt4
29:48 30sOO
_6.7E4
_5.0IT4
_3 . 3£4
_1 . 7E4
O.OEO
Tine
4.9F4
A6.49E3 a2.24E3 A\"f*E*
' 29\ 00 '
29:12' ' ' 29 i 24 '
29: 36'
' 29:48 ' ' ' 30:00 '
_3.9E4
_2.9E4
_1.§£4
_9 . 7E3
O.OJTO
Time
EI+ Voltage SIS 70T Noise: 7 52
,101,3008. 0,0.00%,F,F) ExpsEtCUS
INJ". TIME * 02:17
29:00
AS.
j
/
29:12 29:24
OSES
V"
29:36
-2.2E6
29:48 30. -00
Ll . 8E6
11.3E6
L8.9E5
L4.5E5
• 0 . OEO
Time
File:T966507 #1-443 Acqil-SOV-96 02:14:12 EI+ Voltage SIR 70T JToi.se.-S61
419.8220 F:4 BStm(256,30, -3.0) PKD(5,3,1, 0.10%,2644 .0,0.00%,F,F; Exp-.EPCUS
TRIANGLE LABS Text:23FS-4 HI #39291X1 TWT. TIME = 02:17
100S
so:
60:
40:
20:
o:
,1.51,7
A
. /v
28:12 28:24 28:36 28:48
File:T96S607 #1-443 Aegsl-lTOV-96 02.-14.-12
430.9729 F:4 Exp-.EPCUS
TRIANGLE LABS Text:23FS~4 TLI#39291R1
1003
ao:
60:
40:
20:
o-
_^ 28:21 28:43
fc p.X*c^\ >\ — «^*\ *-«*. iint.yS_l^**l >**™X._
ft r^ ^~^-v^X ^^y^^^'xx N^%
28:12' ' 28:24 ' '28:36' ' 'isU's'
File:T966607 #1-443 Acqsl-OOV-96 02:14:12
479.7165 Fs4 ExpsEPCUS
TRIANGLE LABS Texts 23FB-4 TLH39291S1
100J
SO:
60J
40:
20:
o:
28:19
aa,40
--f\^{ \-'l W^r r^T^ , , . T
28:12 28:24 '28:36' ' '28:48'
29:00
EI+ Voltage
29:01
>^/*s«r«x fj"
^^f ^f ^j^
' 29:00
EH- Voltage
29:04
LAi A_A
29:00
J51.
1
29-12 29:24
sj* 7or
IKT. TTME -
^/N"*"^ "^~^\^«X^
29:12' ' ' 29.-24 '
SIS 70T
INJ. TIKE *
20E7
A
A
V
29:36
02:17
32
l—^V ^*"
29:36'
02:17
(_5,2E6
29:48 30:00
14.2E6
13.1E6
L2.1E6
Ll . 0E6
" 0 . OEO
Time
29:54 1_4.0£6
"™^*Vv_ yml^j^y^^V/r*yx^^^- **
29s 48 30:00
13.2E6
LJ.4E6
Ll . 6E6
L8.0E5
• 0 . OEO
Tine
_1 . 4E4
29:33
29:23 |
^WW\A/\A
29:12 ' " 29:24
Jl A
, — f y ^ i^r
29:36
A !\5 3°A°°
29:48 30:00
Ll.lE4
L8.5E3
L5.6E3
L2.8E3
•O.OEO
Time
319
-------
File:T966607 #1-443 Acgsl-HOV-96 02:14:12 £1+ Voltage SIR 70T Noj.se.-5
423.7766 F:4 SSWB(2S6,30,-3.0) PKD(5,3rl,0.10*,20.0fO.OO*rF,F) Exp:EPCaS
TRIANGLE LABS Text:23FS-4 TLI139291X1 IJKT. TIME - 02:17
100S A3.26E4
28:30 28:36 28:42 28:48 28:54 29iOO 29:06 29:12 29sl8 29:24 29:30
File:T966607 #1-443 Acq:l-SOV-96 02:14:12 EI+ Voltage SIS 70T «oise;155
425.7737 F:4 BSUB(256,30, -3. 0) PKD(5r3,l, 0. 10%, 620. 0, 0. 00%,F,F) Exp:EPCUS
TRIANGLE LABS Text:23FB-4 TLI#33291S1 ISO". TIME = 02:17
1004 A2.39E4
_1.4E4
O.OEO
29:36 29:42 Time
28:30 28:36 28:42 28:48 28:54 29:00 29:06 29:12 29:18 29:24
Tile:T966607 #1-443 Acqsl-SOV-96 02:14:12 EI+ Voltage SIS JOT Noiaei317
435.8169 F:4 BSUB(256,30, -3. 0) PKD(5,3,1, 0.101,1268. 0, 0. 001,F,F) Exp:EPCPS
TRIANGLE LABS Text:23FB-4 TLI#39291R1 UKT. TIME = 02:17
100% A1.Q8E7
801
601
29:30 29:36 29
'.OEO
:42 Time
_3.5E6
'-2.BE6
"-2.1E6
_1. 4E6
7.1E5
28:36 28:42 28:48 28:54 29:00 29:06 29:12 29:18 29:24
FilesT966607 #1-443 Acq:l-ITOV-96 02:14:12 EI+ Voltage SIS 70T Naise:331
437.8140 F:4 BSVB(2S6,30, -3.0) PKS(S,3,1, 0,10%,1324 . 0,0. 00%,-T,F) ExpsEPCffS
TRIANGLE LABS Text:23FB-4 TLI#39291R1 JWJ". TIME = 02:17
100A A1.Q1E7
8 01
601
401
201
29:30 29:36
O.OEO
Time
r3.3E6
-2.6E6
-2.0E6
LI. 3E6
-6.6E5
i i t i
i
28:30 28:36 28:42 28:48 28:54 29:00 29:06 29:12 29:18
File:T966607 #1-443 Acq:l-NOV-96 02:14:12 EI+ Voltage SIB 70T
430.9729 F-.4 Exp:EPCUS
TRIANGLE LABS Text:23FB-4 TZI#39291M1 ZKT. TIME =
JO"* -,D.,Q5fl.^5 -so. AO 29:01 . 29jil7
i 'i t i 'I"!1 r i i"t i '
29:24 29:30
i" i I t i ....... i i1 i i1 ......
29:36 29:42
" " OEO
Time
02:17
sol
601
401
201
01
28:3928i43 28:49
,-4.0E6
-3.2E6
2.4E6
.1.6ES
.8.0E5
28:30 28:36 28:42 28:48 28:54 29:00 29:06 29:12 29:18 29:24 29:30 29:36
-O.QE9
29 • 42 Time
370
-------
File:T966607 01-443 Acqsl-SOV-96 02:14:12 EI+ Voltage SIS JOT SOitte:176
41.7428 T:4 BSOB{256,30, -3.6) PKD(7,2,3,0.10%, 704.0,0.00\rT,f) SxpsEVCUS
TKIA1VSLE LABS Textt23FB-4 TLI#392$1R1 JKT. TIME <= 02:17
1004
29s00 30:00 31:00 32:00
•ile:Ta66607 #1-443 Acgsl-tfOV-SS 02:14:12 EI+ Voltage SIS 70T Koiae:157
443.7399 F:4 BS03(256,30,-3.0) PKD( 7,2,3, 0.10%, 628.0,0. QQ\,FrF) Exp:EPCUS
TRIANGLE LABS Teit:23FB-4 TLI039291K1 IMT. TIME = 02:17
100*
33:00
32:08
33:00
29:00 30:00 31:00
File:T966607 #1-443 Acq:l-HOV-96 02:14:12 EI+ Voltage SIS 70T
430.9729 F:4 Exp:EPCnS
TRIANGLE LABS Text:23FB-4 TLI#39291Rl ' JKT. TJME = 02:17
29117 30:19 31:1131:29 31:52 32:27 32l56 33-16
so|iJ *" •->..«. *^i
flOJ
29:00 30:00 31:00 32:00
File:T966607 #1-443 Acq:l-NOV-96 02:14:12 EI+ Voltage SIK 70T
513.6775 F:4 Ezp:EPCUS
TXIJURLE LABS Zexti33FM-4 TX,I#39291K1 J«T. TIKE ~ 02:17
100*
30:43
33:00
30:07
31:11
33:10
2 .-36
33:
29:00
30s 00'
31.-00'
13Ti
33100
321
-------
rileiT966607 #1-443 Acq:l-NOV-se 02:14:12 EH- Voltage SIS JOT Soieesl3
457.7377 f:4 BSVS( 256,30, -3.0) WO>(7,2,3, 0.10%,52. 0, 0.00%,*-,?,) Exp:EPCUS
TRIANGLE LASS Texts23FB-4 TLI#39291X1 JWJ". TIHE = 02:17
1004 A2.53E5
so:
601
401
20:
'!' *~"pi i i p f i i "I i i 1 r i i ~T—r1 *i I 'i*'" t" | l'" 1 '"i—i i i """ i I "i ^ l"n'^'i ^"f^
31:36 31:42 31:48 31:54 32:00 32:06
fiJe.-2*66S07 #1-443 Acq:l-lTOV-96 02:14:12 EI+ Voltage SIS 70T «oise;B
459.7348 F:4 BSUS(256t30,-3.0) PKD( 7,2,3, 0.10%,32. Ot 0.00*,F,F} Exp:EPCUS
TRIANGLE LABS Text:23FB-4 TX,I#39291S1 IlKT. TIME = 02:17
1001 A3.P5E5
601
40.
01
32:06
2E7
31:36 31:42 31:48 31:54 32:00
F±le:T966607 #1-443 Acq:l-NOV-96 02:14:12 JSJf Voltage SIS 70T No±ae:9
465.7779 F:4 BSUB(256,30, -3. 0) PKD(7,2,3,0.101,36,0,0.00*,F,f'l Elp:EPCUS
TRIANGLE LABS Text:23FB-4 TLI#39291R1 JKT. TIME » 02:17
100* Al.
801
601
40.
201
32:06
31:36 31:42 31:48 31:54 32:00
FileiT966607 #1-443 Acq:l-KOV-96 02:14:12 EI+ Voltage SIS 70T Xoise-.lO
471.7750 f:4 BStJB(256, 30, -3. 0) PKD( 7,2, 3, 0.101,40. 0, 0. 001,F,F) ExpiEFCUS
TRIANGLE LABS Texti23FB-4 TLI#39291R1 IS
-------
, aass 282.3825 Peak top
Height oJi Mdt$ Span fflS ppi
I Systei file naie
' Data file me.
Resotiiion
Group
EPCUS
iQniA&um i
Switching
itf, lasses
fl 293
§ 384
C 386
0 318
E 318
F 31
G 32E
H 528
Cham* I
VOLM
S3
V
K
L
1
H
ij
3
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1
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338
:,^25,
321
-33£
334
348
342
382
2*
358
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^•WA
^7«^
1W/ '*!•
416
S
T
U
V
,3769
368
378
378
413
?m top
^ ^ aa
-------
File:T966607 #1-505 Aeq:l-NOV-96 02:14:12 El-t- Voltage SIR 70T
373.8208 F;3 Exp:EPCUS
Sample Text:23FB-4 TLI#39291R1
100%,
0.
J-^^^
I T| T*I—i—r
25:00 25:12 25:24 25:36 25i48 26:00 26il2 26:24
File:T966607 #1-505 Acq:l-NOV-96 02:14:12 EI+ Voltage SIR 70T
375.8178 F:3 Exp:EPCUS
Sample Text:23FB-4 TLI#39291R1 INJ. TIME
INJ. TIME = 02:17 File Text:23FB-4 TLI#3»
_1.2E4
t6.1E3
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1 (—( !—j.t,—j—j.—,—,—,—|—,—, p.
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25:00 25:12 25:24 25:36 25^48 26100 26il2 26i24
File:T966607 #1-505 Acq:l-NOV-96 02:14:12 EI+ Voltage SIR 70T
383.8639 F:3 Exp:EPCUS
Sample Text:23FB-4 TLI#39291R1 INJ. TIME =
100% 25:13 25:55
50-1
OJ
26i36 26:48 27:00
14.4E3
.O.OEO
Time
25:00 25:12 25:24 25:36 25:48 26:00 26:12 26:24
File:T966607 #1-505 Acq:l-NOV-96 02:14:12 EI+ Voltage SIR 70T
385.8610 F:3 Exp:EPCUS
Sample Text:23FB-4 TLI#39291R1 INJ. TIME =
1001, 25:13 25:55
50.
02:17 File Text:23FB-4 TLI#3»
_3.4E6
26:40
.1.7E6
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Time
26:36 26:48 27:00
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26:40
13.3E6
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25:00 25:12 25:24 25:36 25:48 26:00 26:12 26:24 26:36 26:48 27:00 Time
-------
File:T966607 ttl-443 Aeq;l-NOV-96 02:14:12 EH- Voltage SIR 70T
423.7766 F:4 Exp:EPCUS
Sample Text:23FB-4 TLIf3929lRl
100%
INJ. TIME =
50 J
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28:24 28:36 28:48
File:T966607 #1-443 Acq: l-NOV-96 02:14:12 EI+ Voltage SIR 70T
425.7737 F:4 Exp:EPCUS
Sample Text:23FB-4 TLI#3929lRl _ —^ INJ. TIME =
100%
02:17 File Text:23FB-4 TLI#3»
.1.4E4
16.9E3
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29:00 29:12 29:24 29:36 29:48 30:00 30:12 30:24 Time
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28:24' 28:36 28:48 29:00 29:12 29:24 29:36 29:48 30:00 30:12 30:24 Time
File:T966607 #1-443 Acq: l-NOV-96 02:14:12 EI+ Voltage SIR 70T
435.8169 F:4 Exp:EPCUS
Sample Text:23FB-4 TLI#39291R1 INJ. TIME = 02:17 File Text:23FB-4 TLI#3»
100%
50J
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29; 14
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28:24 28:36 28:48 29:00 29:12 29:24 29:36 29:48 30:00 30:12 30:24 Time
File:T966607 #1-443 Acq: l-NOV-96 02:14:12 EI+ Voltage SIR 70T
437.8140 F:4 Exp:EPCUS
Sample Text:23FB-4 TLI#39291R1 INJ. TIME = 02:17 File Text:23FB-4 TLI#3»
100% 29; 14 _3.3E6
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0.
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28:24 28:36 28:48 29:00 29:12 29:24 29:36 29:48 30:00 30:12 30:24 Time
. ^-
•^
-------
File:T966607 tl-443 Acq:l-NOV-96 02:14:12 EI+ Voltage SIR 70T
441.7428 F:4 Exp:EPCUS
Sample Text:23FB-4 TLI#39291R1 —-==r^ INJ. TIME =
1001. (A4.10E4)
31:00 31:12 31:24 31:36 31:48 32:00 32:12 32:24
File:T966607 #1-443 Acq:l-NOV-96 02:14:12 EI+ Voltage SIR 70T
443.7399 F:4 Exp:EPCUS
Sample Text:23FB-4 TLI#39291R1 _ ^ INJ. TIME =
100%
50.
02:17 File Text:23FB-4 TLIf3»
1.2E4
16.OE3
JLo.QEO
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32:36 32:48 33:00
0.
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31:00 31:12 31:24 31:36 31:48 32:00 32:12 32:24
File:T966607 #1-443 Acq:l-NOV-96 02:14:12 EI+ Voltage SIR 70T
469.7779 F:4 Exp:EPCUS
Sample Text:23FB-4 TLI#39291R1 INJ. TIME =
100% 31;42
LO.OEO
32:36 32:48 33:00 Time
02:17 File Text:23FB-4 TLI#3»
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U_l—!__,—|—, j j—, ,—,—! ! j j ! 1 , ,—, j j—| !_<£, , , , p ] ' |—f—]—,—r—\ 1 1 1—I [—I—I 1—I 1—I—I 1 1—I—f—I—I 1—I 1 1—I—I 1 "I ' t T"""| 1—I 1—r*~ " " UClW
31:00 31:12 31:24 31:36 31:48 32:00 32:12 32:24 32:36 32:48 33:00 Time
File:T966607 #1-443 Acq:l-NOV-96 02:14:12 EI+ Voltage SIR 70T
471.7750 F:4 Exp:EPCUS
Sample Text:23FB-4 TLI#39291R1 INJ. TIME = 02:17 File Text:23FB-4 TLI#3»
100%, 31; 42 4.6E6
12.3E6
.O.OEO
Time
-i—i—i—i—i—i—i—r
31:00 31:12 31:24 31:36 31:48 32:00 32:12 32:24 32:36 32:48 33:00
-------
ci--'-
CALIBRATION
DATA
Triangle Laboratories, Inc.
801 Capiiola Drive P.O. Box 13485
Durham, NC 27713-4411 Research Triangle Park, NC 27709-3485
919-544-5729 fax #919-544-5491
-------
\Et3l- ** V*sis 0 Analytical Services Division
301 Capttola Drive » Durham, North Carofina 27713
Phone: (919) 344-5729 * Fax: (919) 544-5491
Printed: 13:4704/03/96
-------
Isisial Calibration Suaaaary far TF53236
13C"2-=eC3D 122 0.724 0.039 5% 26:01 22:01 30:01 1-483 S
13C12-SXC3F 3~3 1.207 O.OS3 5% 22:36 .24:36 32:36 0.315 5
13C12-3XC3D €78 0.343 0.047 5% 23:19 23:19 30:19 1.20S 5
12C12-HpC3F S73 0.321 0.015 2% 31:17 29:17 35:17 0.431 f
12C12-SpCDD 573 0.770 0,032 4% 32:03 31:03 33:08 1.013 S
13C12-OC3D 0.502 0.028 5% 34:3S 32:3S 3S:36 0.3S4 5
Racovery Standards HF SO ,%RSD 3.T sr/LO RT/HI Racial 3acia2 51
13C12-1234-TCDD 1.000 0.000 0% 21=15 0.797 S
13C12-axCSD 789 1.000 0.000 0% 29:37 1.207 S
»•""• End of Reoorr ***
saga
Trtangia Laboratories, Inc.3 Analytical Sarvicas Division
801 Capttola Drive • Curtain, North Carolina 27713 Printed: 13:47 CW03/S6
Phone: (919) 344-5729 - Fax: (919) 544-5491
T75
-------
Date: 11/06/96
TRIANGLE LABORATORIES, INC.
Continuing Calibration for T966704
Method : M237
Operator
• MM
Init Calibration • T
ICal Date
Analyte Summary
Name
Total MCDF
Total MCDD
Total DCDF
Total DCDD
Total TriCDF
Total TriCDD
2378-TCDF
TOTAL TCDF
2378-TCDD
TOTAL TCDD
12378-PeCDF
23478-PeCDF
TOTAL PeCDF
12378-PeCDD
TOTAL PeCDD
123478-HxCDF
123678-HxCDF
234678-HxCDF
123789-HxCDF
TOTAL HxCDF
123478-HxCDD
123678-HxCDD
'FR'n.Rfi
• 03/28/96
RF Ratio
0.
0.
0.
0.
0.
0.
1.
1.
1.
1.
1.
0.
1,
1.
1.
1.
1.
1.
1.
1.
0.
1.
1&2
000
000
000
000
000
000
036 0.81
036 0.81
154 0.80
154 0.80
048 1.54
974 1.54
Oil 1.54
231 1.57
231 1.57
116 1.25
370 1.24
136 1.25
028 1.25
162 1.25
903 1.24
Oil 1.23
Instrument -
Std Cone
RT RT Rel . RT
. : T
ICal
RF
•50.00
Delta
RF
%D
Lo/High
0:
9:
0:
10
2:
10
3:
11
6:
13
8:
14
12
17
13
17
17
23
19
22
23
26
24
26
01
26
01
:13
26
:26
13
:13
26
:26
13
:13
:48 15:28 1.0022
:34
:43 16:14 1.0010
:35
:37 20:42 1.0008
:03
21:43 1.0500
:33 22:11 1.0008
:56
:50 25:08 0.9960
:51
25:15 1.0007
25:51 1.0244
26:36 1.0542
:28 26:01 0.9974
:32
26:06 1.0006
1
1
0
1
0
0
1
1
1
1
1
1
1
1
1
1
1
1
0
1
0
1
.365
.734
.598
.188
.594
.289
.090
.090
.206
.206
.086
.122
.104
.251
.251
.088
.353
.094
.985
.130
.914
.000
-1.
-1.
-0.
-1.
-0.
-0.
-0.
-0.
-0.
-0.
-0.
-0.
-0.
-0.
-0.
0.
0.
0.
0.
0.
-0.
0.
365
734
598
188
594
289
054
054
052
052
038
148
093
020
020
028
017
042
043
032
Oil
Oil
100,
100.
100.
100.
100.
100.
-4.
-4.
-4.
-4.
-3.
-13.
-8.
-1.
-1
2.
1,
3.
4.
2
-1
1
. 0%
. 0%
. 0%
.0%
,0%
0%
9%
9%
3%
.3%
5%
.2%
.4%
.6%
.6%
.6%
.2%
.8%
.3%
.9%
.2%
.1%
Page 1
Triangle Laboratories, Inc.® Analytical Services Division
801 Capitola Drive • Durham, North Carolina 27713
Phone: (919) 544-5729 • Fax: (919) 544-5491
Printed: 22:39 11/06/96
-------
Date: 11/06/96
TRIANGLE LABORATORIES, INC,
Continuing Calibration tor T966704
123789-HxCDD
TOTAL HxCDD
1234678-HpCDF
1234789-HpCDF
TOTAL HpCDF
1234678-HpCDD
TOTAL HpCDD
OCDF
OCDD
1.002
0.972
1.662
1.182
1.422
0.951
0.951
1.290
1.029
1.
1.
1.
1.
1.
1.
1.
0,
0.
24
23
07
07
07
,03
,03
,90
.85
28
29
28
29
27
35
27
35
26:25
:05 28:15
:41
29:30
:23 29:11
:21
:39 31:44
:39
:39 31:40
-.39
1.0128
1.0006
1.0449
1.0006
1.0026
1.0005
Other Standard Summary
Name
RF
Ratio
1&2
37C1-TCDD
13C12-PeCDF 234
13C12-HXCDF 478
13C12-HXCDF 234
13C12-HXCDF 789
13C12-HXCDD 478
13C12-HpCDF 789
Internal Standard
Same
0.951
0.891
0.976
0.992
0.817
0.894
0.869
1.
0
0
0
1
0
.51
.51
.51
.50
.22
.43
RT RT
Rel. RT
1.036
0.983
1.764
1.132
1.448
0.961
0.961
1.180
1.017
ICal
RF
-0
-0
-0
0
-0
-0
-0
0
0
.034
.011
.102
.050
.026
.010
.010
.110
.012
-3.
-1.
-S.
4 .
-1.
-1.
-1,
9.
1.
3%
1%
8%
4%
8%
0%
0%
3%
2%
Delta
RF
%D
Lo/High
14
18
16
24
26
32
:13 16:14
-.13
:41 21:42
:41
25:07
25:50
26:35
26:00
:14 29:30
:14
1.0010
1.0492
0.9954
1.0238
1.0535
0.9968
1.0449
Summary
RF
Rat to
1S2
13C12-2378-TCDF
13C12-2378-TCDD
13C12-PeCDF 123
13C12-PeCDD 123
13C12-HXCDF 678
13C12-HxCDD 678
1.380
1.071
1.055
0.579
1.215
0.980
0
0
1
1
0
1
.72
.80
.49
.48
.48
.21
Rt RT
Rel. Rf
0.934
1.018
0.933
0.949
0.772
0.899
0.789
ICal
RF
0
-0
0
0
0
-0
0
.017
.127
.043
.043
.045
.005
.080
1,
-12.
4,
4.
5.
-0
10
,8%
,5%
,6%
.6%
.8%
.6%
.1%
Delta
8F
*D
Lo/Hifh
14
16
14
18
16
24
18
26
21
29
25
27
:26 15:26
:26
:13 16:13
:13
:41 20:41
:41
:10 22:10
:10
:14 25:14
:14
:05 26:05
:05
1.0000
1.0000
1.0000
1.0000
1.0000
1.0000
1.266
1.049
1.207
0.709
1.207
0.943
0
0
-0
-0
0
0
,114
.022
.152
.130
.008
.037
9
2
-12
-18
0
3
.0%
.1%
.6%
.3%
.7%
.9%
Page 2
Triangle Laboratories, Inc.® Analytical Services Division
801 Capitola Drive • Durham, North Carolina 27713
Phone: (919) 544-5729 • Fax: (919) 544-5491
Printed: 22:39 11/06/96
-------
Date: 11/06/96 TRIANGLE LABORATORIES, INC.
Continuing Calibration for T966704
13C12-HpCDF 678 0.872 0.44 26:14 28:14 1.0000 0.821 0.051 6.2%
32:14
13C12-HpCDD 678 0.90S 1.01 28:10 29:10 1.0000 0.770 0.138 17.9%
30:10
13C12-OCDD 0.667 0.87 31:30 31:39 1.0000 0.602 0.065 10.8%
31:50
Recovery Standard Summary ICal Delta
Name RF Ratio RT RT Rel. RT RF RF %D
1&2 Lo/High
13C12-1234-TCDD 1.000 0.80 16:00 0.9866 1.000 0.000 0.0%
13C12-HxCDD 789 1.000 1.22
26:24 1.0121 1.000 0.000 0.0%
QC Front End Check:
1.0542
Page
Triangle Laboratories, Inc.® Analytical Services Division
801 Capitola Drive • Durham, North Carolina 27713
Phone: (919) 544-5729 • Fax: (919) 544-5491
Printed: 22:39 11/06/96
-------
Date: 11/08/96
TRIANGLE LABORATORIES, INC.
Continuing Calibration for T966758
Operator , . . .
Xnifc Calibration.
ICal Date
Analyte Summary
Name
J.A/ WW
• MM
/ ^"
: TF53286
• 03/28/96
RF
Ratio
1&2
fotal HCDF
Total MCDD
Total DCDF
fotal DCDD
Total TriCDF
fotal TriCDD
2378-TCDF
TOTAL TCDF
2378-TCDD
TOTAL TCDD
12378 -PeCDF
23478- PeCDF
TOTAL PeCDF
12378-PeCDD
TOTAL PeCDD
123478 -HxCDF
123678-HxCDF
234678-HxCDF
123789-HxCDF
TOTAL HxCDF
123478-HxCDD
123678-HxCDD
0.000
0.000
0.000
0.000
0.000
0.000
1.077
1.077
1.131
1.131
1.076
1.061
1.068
1.175
1.175
1.094
1.395
1.076
0.984
1.135
0.838
0.998
0.
0.
0.
0.
1.
1.
1.
1.
1.
1.
1.
1.
1.
1.
1.
1.
81
81
78
78
53
51
52
56
56
26
27
24
26
26
21
21
RT
to/High
0:01
9:25
0:01
10:10
2:25
10:25
3:10
11:10
6:25
13:25
8:10
14:10
12:45
17:30
13:39
17:30
17:32
22:59
19:29
22:53
23:46
26:48
24:25
26:29
Page
Instrument
Std . Cone
. . : T
50.00
ICal Delta
Rf Rel. RT
15:26 1.0011
16:11 1.0010
20:39 1.0008
21:40 1.0501
22:09 1.0015
25:06 0.9960
25:13 1.0007
25:49 1.0245
26:34 1.0542
25:59 0.9974
26:04 1.0006
1
RF RF %D
1.365 -1.365 100.0%
1.734 -1.734 100.0% ""*~ p1 »^" ^^^"
( ^***"**"*^
0.598 -0.598 100.01 -«-•— -""""^
*— — -*"^
1.188 -1.188 100.0%
0.594 -0.594 100.0%
0.289 -0.289 100.0%
1.090 -0.013 -1.2%
1.090 -0.013 -1.2%
1.206 -0.075 -6.2%
1.206 -0.075 -6.2%
1.086 -0.010 -0.9%
1.122 -0.061 -5.5%
1.104 -0.036 -3.2%
1.251 -0.076 -6.1%
1.251 -0.076 -6.1%
1.088 -0.004 -0.4%
1.353 0.042 3.1%
1.094 -0.018 -1.6%
0.985 -0.001 -0.1%
1.130 0.005 0.4%
0.914 -0.076 -8.3%
1.000 -0.002 -0.2%
Triangle Laboratories, Inc.® Analytical Services Division
801 Capitola Drive • Durham, North Carolina 27713
Phone: (919) 544-5729 • Fax: (919) 544-5491
Printed: 14:12 11/08/96
111
-------
Date: 11/08/96
TRIANGLE LABORATORIES,
Continuing Calibration
123789-HxCDD
TOTAL HxCDD
1234678-HpCDF
1234789-HpCDF
TOTAL HpCDF
1234678-HpCDD
TOTAL HpCDD
OCDF
OCDD
Other Standard
Name
37C1-TCDD
13C12-PeCDF 234
13C12-HxCDF 478
13C12-HxCDF 234
13C12-HXCDF 789
13C12- HxCDD 478
13C12-HpCDF 789
0.976
' 0.937
1.680
1.127
1.404
0.960
0.960
1.240
1.000
Summary
RF
0.923
0.941
0.956
0.946
0.776
0.853
0.808
1.19
1.20
1.04
1.05
1.05
1.02
1.02
0.92
0.86
Ratio
1&2
1.56
0.52
0.51
0.51
1.24
0.42
28:02
29:39
28:21
29:19
27:38
35:38
27:38
35:38
RT
Lo/High
14:10
18:10
16:38
24:38
26:12
32:12
26:
28:
29:
29:
31:
31:
RT
16:
21:
25:
25:
26:
25:
29:
23
13
29
09
43
39
INC.
for T966758
1
1
1
1
1
1
.0128
.0006
.0455
.0000
.0026
.0005
Rel. RT
11
39
05
49
34
58
29
1
1
0
1
1
0
1
.0010
.0493
.9954
.0245
.0542
.9968
.0455
Internal Standard Summary
Name
13C12-2378-TCDF
13C12-2378-TCDD
13C12-PeCDF 123
13C12-PeCDD 123
13C12-HxCDF 678
13C12 -HxCDD 678
RF
1.327
1.057
0.983
0.499
1.304
0.996
Ratio
1&2
0.74
0.79
1.50
1.50
0.50
1.23
RT
Lo/High
14:25
16:25
14:10
18:10
16:38
24:38
18:07
26:07
21:12
29:12
25:03
27:03
Page
RT
15:
16:
20:
22:
25:
26:
2
Rel . RT
25
10
38
07
12
03
1
1
1
1
1
1
.0000
.0000
.0000
.0000
.0000
.0000
1.036
0.983
1.764
1.132
1.448
0.961
0.961
1.180
1.017
ICal
RF
0.934
1.018
0.933
0.949
0.772
0.899
0.789
ICal
RF
1.266
1.049
1.207
0.709
1.207
0.943
-0.060
-0.046
-0.084
-0.005
-0.044
-0.001
-0.001
0.060
-0.017
Delta
RF
-0.011
-0.077
0.023
-0.003
0.004
-0.046
0.019
Delta
RF
0.061
0.008
-0.224
-0.210
0.097
0.053
-5.
-4 .
-4.
-0.
-3,
-0.
-0.
5.
-1.
%D
-1.
-7.
2.
-0,
0.
-5,
2.
%D
4.
0.
-18,
-29.
8.
5.
8%
6%
8%
4%
. 1%
1%
,1%
0%
.6%
.1%
.6%
.5%
.3%
.5%
,1%
,4%
,8%
,7%
.5%
,6%
, 0%
.6%
Triangle Laboratories, Inc.© Analytical Services Division
801 Capitola Drive«Durham, North Carolina 27713
Phone: (919) 544-5729 • Fax: (919) 544-5491
Printed: 14:1211/08/96
JT ^
-------
Date: 11/08/96 IRIANGLE LABORATORIES, INC.
Continuing Calibration for T966758
13C12-HpCDF 678 0.766 0,43 26:12 28:12 1.0000 0,821 -0.055 -6.6%
32:12
13C12-HpCDD 678 0.671 1.04 28:09 29:09 1.0000 0.770 -0.099 -12.9%
30:09
13C12-OCDD 0.499 0.86 31:28 31:38 1.0000 0.602 -0.103 -17.1%
31:48
Recovery Standard Summary ICal Delta
Name RF Ratio RT RT Rel. RT RF RF %D
1&2 Lo/High
13C12-1234-TCDD 1.000 0.80 15:57 0.9866 1.000 0.000 0.0%
13C12-HXCDD 789 1.000 1.20
26:22 1.0122 1.000 0.000 O.Oi
QC Front End Check:
2.3142
Page
Triangle Laboratories, Inc.® Analytical Services Division
801 Capitola Drive • Durham, North Carolina 27713
Phone: (919) 544-5729 • Fax: (919) 544-5491
Printed: 14:12 11/08/96
-------
PACIFIC ENVIRONMENTAL SERVICES. INC.
Central Park West
5001 South Miami Boulevard, P.O. Box 12077
Research Triangle Park, North Carolina 27709-2077
(919)941-0333 FAX: (919) 941-0234
Particulate Matter Residue Calculations
Lab Sample ID No.
101
102
103
104
105
106
107
108
109
110
111
112
113
114
115
116
117
118
119
120
121
122
123
124
125
126
127
128
129
130
131
132
133
134
135
136
137
138
139
140
141
142
143
144
145
Field Sample No
M29-1-A-AR2
M29-1-A-F1
M29-1-B-AR2
M29-1-B-F1
M29-2-A-AR2
M29-2-A-F1
M29-2-B-AR2
M29-2-B-F1
M29-3-A-AR2
M29-3-A-F1
M29-3-B-AR2
M29-3-B-F1
M29-4-AR2
M29-4-F1
M29-5-AR2
M29-5-F1
M29-6-AR2
M29-6-F1
M29-7-AR2
M29-7-F1
M29-FB-AR2
M29-FB-F1
M29-RB-AR2
M29-RB-F1
M29-10-AR2
M29-10-F1
M29-11-AR2
M29-11-F1
M29-12-AR2
M29-12-F1
M29-13-I-AR2
M29-13-I-F1
M29-13-I-BH Filtrate
M29-13-O-AR2
M29-13-O-F1
M29-14-I-AR2
M29-14-I-F1
M29-14-O-AR2
M29-14-O-F1
M29-15-I-AR2
M29-15-I-F1
M29-15-0-AR2
M29-15-O-F1
M29-FB-I-AR2
M29-FB-I-F1
Blank
Wash
Volume
(L)
0.1902
0.1902
0.1902
0.1902
0.1902
0.1902
0.1902
0.1902
0.1902
0.1902
0.1902
0.1902
0.1902
0.1902
0.1902
0.1902
0.1902
0.1902
0.1902
0.1902
0.1902
0.1902
0.1902
0.1902
0.1902
0.1902
0.1902
0.1902
0.1902
0.1902
0.1902
0.1902
0.1902
0.1902
0.1902
0.1902
0.1902
0.1902
0.1902
0.1902
0.1902
0.1902
0.1902
0.1902
0.1902
Blank
Residue
(g)
0.0013
0.0013
0.0013
0.0013
0.0013
0.0013
0.0013
0.0013
0.0013
0.0013
0.0013
0.0013
0.0013
0.0013
0.0013
0.0013
0.0013
0.0013
0.0013
0.0013
0.0013
0.0013
0.0013
0.0013
0.0013
0.0013
0.0013
0.0013
0.0013
0.0013
0.0013
0.0013
0.0013
0.0013
0.0013
0.0013
0.0013
0.0013
0.0013
0.0013
0.0013
0.0013
0.0013
0.0013
0.0013
Blank
Concentration
(9/L)
0.0066
0.0066
0.0066
0.0066
0.0066
0.0066
0.0066
0.0066
0.0066
0.0066
0.0066
0.0066
0.0066
0.0066
0.0066
0.0066
0.0066
0.0066
0.0066
0.0066
0.0066
0.0066
0.0066
0.0066
0.0066
0.0066
0.0066
0.0066
0.0066
0.0066
0.0066
0.0066
0.0066
0.0066
0.0066
0.0066
0.0066
0.0066
0.0066
0.0066
0.0066
0.0066
0.0066
0.0066
0.0066
Sample
Wash
Volume
(L)
0.2023
0.0000
0,2153
0.0000
0.2374
0,0000
0.1679
0.0000
0.2111
0.0000
0.1706
0.0000
0.2073
0.0000
0.1684
0.0000
0.1850
0.0000
0.1893
0.0000
0.1965
0.0000
0.1902
0.0000
0.2844
0.0000
0.2758
0.0000
0.2812
0.0000
0.6018
0.0000
0.0000
0.1721
0.0000
0,5757
0.0000
0.1991
0.0000
0.6297
0.0000
0.1921
0.0000
0.1854
0.0000
Sample
Residue
Weight
(g)
0.0143
0.3804
0.0235
0.3398
0.0355
0.5511
0.0100
0.3402
0.0393
0.3734
0.0124
0.2875
0.0184
0.1187
0.0172
L0.1081
0.0126
0.1147
0.0178
0.1210
0.0050
0.0150
0.0012
0.0030
0.2485
0.4907
0.1658
0.3112
0.2366
0.4600
29.9650
1.3226
1.1033
0.0276
0.1175
32.4053
0.7521
0.0104
0.1004
28.2634
1.5215
0.0139
0.0988
0.0082
0.0007
Blank
Correction
(g)
0.0013
0.0000
0.0014
0.0000
0.0016
0.0000
0.0011
0.0000
0.0014
0.0000
0.0011
0.0000
0.0014
0.0000
0.0011
0.0000
0.0012
0.0000
0.0012
0.0000
0.0013
0.0000
0.0013
0.0000
0.0019
0.0000
0.0018
0.0000
0.0018
0.0000
0.0040
0.0000
0.0000
0.0011
0.0000
0.0038
0.0000
0.0013
0.0000
0.0041
0.0000
0.0013
0.0000
0.0012
0.0000
Net
Residue
Weight
(g)
0.0129
0.3804
0.0221
0.3398
0.0339
0.5511
0.0089
0.3402
0.0379
0.3734
0.0113
0.2875
0.0170
0.1187
0.0161
0.1081
0.0113
0.1147
0.0165
0.1210
0.0037
0.0150
0.0000
0.0030
0.2467
0.4907
0.1640
0.3112
0.2348
0.4600
29.9610
1.3226
1.1033
0.0265
0.1175
32.4015
0.7521
0,0091
0.1004
28.2593
1.5215
0.0126
0.0988
0.0070
0.0007
Residue
Weight
Run
(g)
0.3933
0.3619
0.5850
0.3491
0.4113
0.2988
0.1358
0.1242
0.1260
0.1375
0.0187
0.0030
0.7374
0.4752
0.6949
32.3869
0.1440
33.1536
0.1095
29.7807
0.1113
0,0076
-------
Q PACIFIC ENVIRONMENTAL SERVICES. INC.
Front Half Wash Bottle Data
Central Park West
5001 South Miami Boulevard, P.O. Box 12077
Research Triangle Park, North Carolina 27709-2077
(919)941-0333 FAX: (919) 941-0234
Lab Sample ID No.
101
102
103
104
105
106
107
108
109
110
111
112
113
114
115
116
117
118
119
120
121
122
123
124
125
126
127
128
129
130
131
132
133
134
135
136
137
Field Sample ID No
M29-1-A-AR2
M29-1-A-F1
M29-1-B-AR2
M29-1-B-F1
M29-2-A-AR2
M29-2-A-F1
M29-2-B-AR2
M29-2-B-F1
M29-3^A-AR2
M29-3-A-F1
M29-3-B-AR2
M29-3-8-F1
M29-4-AR2
M29-4-F1
M29-5-AR2
M29-5-F1
M29-6-AR2
M29-6-F1
M29-7-AR2
M29-7-F1
M29-FB-AR2
M29-FB-F1
M29-RB-AR2
M29-RB-F1
M29-10-AR2
M29r10-F1
M29-11-AR2
M29-11-F1
M29-12-AR2
M29-12-F1
M29-13-I^R2
M29-13-I-F1
M29-13-I-BH Filtrate
M29-13-O-AR2
M29-13-O-F1
M29-14-I-AR2
M29-14-I-F1
Filter
Number
301633-301666
1669-301680-301655
301664-301663
301668
301670-301677
301681
301672
301665
301448
301676
301576
1645-301650-301562
301486
301679
301643
301646-301647
301654
301673-301637
Description
Run 1 - Outlet A FH
Run 1 - Outlet A Filter(s)
Run 1 - Outlet B FH
Run 1 - Outlet B Fi!ter(s)
Run 2 -Outlet A FH
Run 2 - Outlet A Filter(s)
Run 2 - Outlet B FH
Run 2 - Outlet B Filter(s)
Run 3 -Outlet A FH
Run 3 - Outlet A Filters)
Run 3 - Outlet B FH
Run 3 - Outlet B Filters)
Run 4 - FH
Run 4 - Filters)
Run5-FH
Run 5 - Filter(s)
Run 6 - FH
Run 6 - Filterfs)
Run 7 - FH
Run 7 - Filter(s)
Field Blank - FH
Field Blank - Filters
Reagent Blank - FH
Reagent Blank - Filters
Run10-FH
Run 10 - Filters)
Run11-FH
Run11-Filter(s)
Run12-FH
Run 12 - Filter(s)
Run 13 -Inlet FH (2 Bottles)
Run 13 -Inlet Filters)
Run 13 - Inlet Back Half Filtrate
Run 13 - Outlet FH
Run 13 -Outlet Filters)
Run 14 - Inlet FH
Run 14 - Inlet Filter(s)
Solvent
Acetone
Acetone
Acetone
Acetone
Acetone
Acetone
Acetone
Acetone
Acetone
Acetone
Acetone
Acetone
Acetone
Acetone
Acetone
Acetone
Acetone
Acetone
Initial
Bottle
Weight
(9)
256.9
267.2
305.5
248.4
263.1
231.0
260.8
229.2
242.5
246.4
251.4
269.2
343.1
335.4
339.1
885.7
232.7
673.7
Final
Bottle
Weight
(9)
168.0
168.0
188.8
186.7
167.2
167.2
167.9
167.1
167.3
167.8
167.1
189.9
189.2
188.3
187.7
575.5
167.7
407.9
Difference
(g)
88.9
99.2
116.7
61.7
95.9
63.8
92.9
62.1
75.2
78.6
84.3
79.3
153.9
147.1
151.4
310.2
65.0
265.8
1/Density
of
Solvent
(ml/g)
1.263
1.263
1.263
1.263
1.263
1.263
1.263
1.263
1.263
1.263
1.263
1.263
1.263
1.263
1.263
1.263
1.263
1.263
Field
Sample
Volume
(ml)
112.3
125.3
147.4
77.9
121.1
80.6
117.3
78.4
95.0
99.3
106.5
100.2
194.4
185.8
191.2
391.8
82.1
335.7
Lab
Wash
Volume
(ml)
90
90
90
90
90
90
90
90
90
iO
90
90
90
90
90
210
90
240
. Total
Wash
Volume
(ml)
202.3
215.3
237.4
167.9
211.1
170.6
207.3
168.4
185.0
189.3
196.5
190.2
284.4
275.8
281.2
601.8
172.1
575.7
-------
PACIFIC ENVIRONMENTAL SERVICES. INC.
Front Half Wash Bottle Data
Central Park West
5001 South Miami Boulevard, P.O. Box 12077
Research Triangle Park, North Carolina 27709-2077
(919) 941-0333 FAX: (919) 941-0234
Lab Sample ID No.
138
139
140
141
142
143
144
145
Field Sample ID No
M29-14-C^AR2
M29-14-O-F1
M29-15-I-AR2
M29-15-I-F1
M29-15-O-AR2
M29-15-O-F1
M29-FB-I-AR2
M29-FB-I-F1
Filter
Number
-
301648
-
301644-301639
-
301624
-
301628
Description
Run 14 - Outlet FH
Run 14 - Outlet Filter(s)
Run 15- Inlet FH
Run 15- Inlet Filter(s)
Run 15- Outlet FH
Run 15- Outlet Filter(s)
Field Blank - Inlet FH
Field Blank - Inlet Filter(s)
Solvent
Acetone
Acetone
Acetone
Acetone
Initial
Bottle
Weight
(g)
253.2
808.8
248.4
480.5
Final
Bottle
Weight
(9)
166.8
405.2
167.6
405.0
Difference
(g)
86.4
403.6
80.8
75.5
1 /Density
of
Solvent
(ml/g)
1.263
1.263
1.263
1.263
Field
Sample
Volume
(ml)
109.1
509.7
102.1
95.4
Lab
Wash
Volume
(ml)
90
120
90
90
Total
Wash
Volume
(ml)
199.1
629.7
192.1
185.4
fa-
-------
O PACIFIC ENVIRONMENTAL SERVICES. INC.
Method 8 Final Weights
Central Park West
5001 South Miami Boulevard, P.O. Box 12077
Research Triangle Park, North Carolina 27709-2077
(919) 941-0333 FAX: (919) 941-0234
Project Number:
Date:
Time
R.H (%)
Temp f F)
Std, Wt. (g)
Analyst
Lab Sample ID No.
101
102
103
104
105
106
107
108
109
110
111
112
113
114
115
116
117
118
119
120
121
122
123
124
125
126
127
128
129
130
131
132
133
S401.004
Field Sample ID No
M29-1-A-AR2
M29-1-A-F1
M29-1-B-AR2
M29-1-B-F1
M29-2-A-AR2
M29-2-A-F1
M29-2-B-AR2
M29-2-B-F1
M29-3-A-AR2
M29-3-A-F1
M29-3-B-AR2
M29-3-B-F1
M29-4-AR2
M29-4-F1
M29-5-AR2
M29-5-F1
M29-6-AR2
M29-6-F1
M29-7-AR2
M29-7-F1
M29-FB-AR2
M29-FB-F1
M29-RB-AR2
M29-RB-F1
M29-10-AR2
M29-10-F1
M29-11-AR2
M29-11-F1
M29-12-AR2
M29-12-F1
M29-13-I-AR2
M29-13-1-F1
M29-13-I-BH Fittrate
Item Weighed: Beakers & filters
I 11/6/96
10:50 AM
I 99,9998
MDM
1st
104.2389
103.7310
101.6727
99.5927
106.4132
96.9187
105.7101
108.3197
110.2036
102.1906
106.0027
109.1937
108.4614
109.4856
105.1670
11/7/96
8:45 AM
100.0000
MDM
2nd
97.8017
104.2401
108.3085
103.7323
101.6739
113.8523
99.5939
105.8440
106.4142
102.0415
96.9194
104.7973
105.7105
110.9876
108.3202
1 12.7374
110.2038
103.9630
102.1907
104.2644
106.0028
103.8626
109.1937
111.5504
108.4628
118.2163
109.4859
105.3342
105.1684
117,1491
11/7/96
3:20 PM
99.9999
MDM
3rd
97.8015
104.2393
108.3084
103.7315
101.6735
113.8521
99.5933
105.8427
106.4137
102.0407
96.9187
104.7963
110.9871
112.7367
103.9620
104.2639
103.8624
111.5506
108.4629
118.2159
105.3342
105.1686
117.1491
11/8/96
8:50 AM
99.9999
MDM
4th
104.2399
103.7324
105.4629
99.5947
105.8431
102.0414
96.9201
104.7968
112.7379
103.9627
133.3020
11/8/96
3:15 PM
99.9998
MDM
5th
104.2409
103.7329
105.4638
99.5956
102.0416
96.9202
112.7379
103.9632
133.3637
11/11/96
8:35 AM
100.0002
MDM
6th
104.2396
105.4631
99.5937
133.4135
102.5550
11/11/96
3:25 PM
100.0000
MDM
7th
104.2385
105.4625
99.5941
133.4252
102.5554
11/12/96
9:40 AM
100.0001
MDM
8th
104.2400
105.4628
133.4326
Difference
(mg)
0.2
-1.5
0.1
-0.5
-0.3
0.4
0.2
-0.4
-0.4
0.5
-0.2
-0.1
-0.5
-0.4
0.5
-0.5
0.0
-0.2
-0.5
-0.1
0.5
-0.1
0.2
0.0
-0.2
-0.1
0.4
-0.3
0.0
-0.2
-7.4
0.0
-0.4
Average
Beaker
Weight
(Final)
{g)
97.8016
104.2393
108.3085
103.7327
105.4627
101.6737
113.8522
99.5939
105.8429
106.4140
102.0415
96.9202
104.7966
105.7103
110.9874
108.3200
112.7379
110.2037
103.9630
102.1907
104.2642
106.0028
103.8625
109.1937
111.5505
108.4629
118.2161
109.4858
105.3342
105.1685
133.4289
117.1491
102.5552
Average
Beaker
Weight
(Initial)
(g)
97.7874
103.8590
108.2850
103.3929
105.4272
101.1226
113.8422
99.2537
105.8036
106.0406
102.0291
96.6326
104.7782
105.5916
110.9702
108.2119
112.7254
110.0890
103.9452
102.0697
104.2592
105.9878
103.8613
109.1908
111.3020
107.9722
118.0503
109.1746
105.0976
104.7085
103.4766
115.8266
1014519
Sample
Residue
Weight
(9)
0.0143
0.3803
0.0235
0.3398
0.0355
0.5511
0.0100
0.3402
0.0393
0.3734
0.0124
0.2875
0.0184
0,1187
0,0172
0.1081
0.0126
0.1147
0.0178
0.1210
0.0050
0.0150
0.0012
0,0030
0.2485
0.4907
0.1658
0.3112
0.2366
0.4600
29.9523
1,3226
1.1033
-------
O PACIFIC ENVIRONMEMTAL SERVICES. INC.
Method 5 Final Weights
Centra! Park West
5001 South Miami Boulevard, P.O. Box 12077
Research Triangle Park, North Carolina 27709-2077
(919) 941-0333 FAX: (919) 941-0234
11/6/96
10:50 AM
99,9998
MDM
Lab Sample ID No.
Field Sample ID No
1st
11/7/96
8:45 AM
100.0000
MDM
2nd
11/7/96
3:20 PM
99.9999
MDM
3rd
11/8/96
8:50 AM
99.9999
MDM
4th
11/8/96
3:15 PM
99.9998
MDM
5th
11/11/96
8:35 AM
100.0002
MDM
6th
11/11/96
3:25 PM
100.0000
MDM
7th
11/12/96
9:40 AM
100.0001
MDM
8th
Difference
(mg)
Average
Beaker
Weight
(Final)
(9)
Average
Beaker
Weight
(Initial)
(g)
Sample
Residue
Weight
(9)
134
M29-13-0-AR2
106.6747
106.6746
0.1
106.6747
106.6471
0.0276
135
M29-13-O-F1
105.1409
105.1412
-0.3
105.1411
105.0236
0.1175
136
M29-14-I-AR2
134.5863
134.6009
134.6128
-11,9
134.6069
102.2140
32.3929
137
M29-14-I-F1
115.9192
115.9191
0.1
115.9192
115.1671
0.7521
138
M29-14-O-AR2
101.1179
101.1178
0.1
101.1179
101.1075
0.0104
139
M29-14-O-F1
115.6937
115.6937
0.0
115.6937
115.5933
0.1004
140
M29-15-I-AR2
153.2699
150.2977
3.0
116.0163
-116.0163
141
M29-15-I-F1
109,1904
109.1905
-0.1
109.1905
107.6690
1.5215
142
M29-15-0-AR2
98.5116
98.5117
-0.1
98.5117
98.4978
0.0139
143
M29-15-O-F1
111.1698
111.1694
0.4
111.1696
111.0709
0.0988
144
M29-FB-I-AR2
99.6390
99.6396
99.6390
99.6385
0.5
99.6388
99.6306
0.0082
145
M29-FB-I-F1
102.7567
102.7568
-0.1
102.7568
102.7561
0.0007
146
0.0
100.7784
-------
PACIFIC ENVIRONMENTAL SERVICES. INC.
Method 5 Final Weights
Central Park West
5001 South Miami Boulevard, P.O. Box 12077
Research Triangle Park, North Carolina 27709-2077
(919) 941-0333 FAX: (919) 941-0234
Project Nu
Date:
Time
R.H {%)
Temp (°F)
Std. m, (g)
Analyst
Lab Sampl
102
131
136
140
S401.004
Field Sampl
M29-1-A-F
M29-13-I-A
M29-14-I-A
M29-15-I-A
Item Weighed: Beakers & filters
11/12/96
9:40 AM
100.0001
MDM
8th
104.2400
133.4326
134.6128
150.2977
11/13/96
9:50 AM
99.9997
MDM
9th
104.2386
133.4506
134.6257
147.2433
11/13/96
3:50 PM
99,9999
MDM
10th
146.5637
11/14/96
10:30 AM
100.0000
MDM
11th
144,3347
11/14/96
4:35 PM
99.9997
MDM
12th
144.2247
Difference
(mg)
1.4
-18.0
-12.9
110.0
Average
Beaker
Weight
(Final)
(g)
104.2393
133,4416
134.6193
144.2797
Average
Beaker
Weight
(Initial)
(g)
103.8590
103.4766
102.2140
116.0163
Sample
Residue
Weight
(g)
0.3804
29.9650
32,4053
28.2634
-------
Final Wts,
ENVIRONMENTAL SERVICES. INC.
Method 5 Final Weights
Lab Sample ID No.
Field Sample No
1st
2nd
3rd
4th
5th
6th
7th
Difference (mg)
Avg. Tare Wt, (g)
101
M29-1-A-AR2
, #<>($
#DIV/0!
102
M29-1-A-F1
#DIV/0!
103
M29-1-B-AR2
160-3064;
#D!V/Q!
104 f
M29-1-B-F1
\OM3lO
#DIV/0!
105
M29-2-A-AR2
#DIV/0!
106 -f
M29-2-A-F1
#DIV/0!
107
M29-2-B-AR2
#DIV/0!
108
M29-2-B-F1
#D1V/OI
109
M29-3-A-AR2
#DIV/0!
110
M29-3-A-F1
#DIV/0!
111
M29-3-B-AR2
#DIV/0!
112
M29-3-B-F1
#DIV/0!
113*
M29-4-AR2
\OCkTf\69
#DIV/0!
1144
M29-4-F1
#DIV/0!
M29-5-AR2
#DIV/0!
116
M29-5-F1
#DIV/0!
117*
M29-6-AR2
#DIV/0!
M29-6-F1
#DIV/0!
M29-7-AR2
#DIV/0!
120:*-
M29-7-F1
#DIV/01
121
M29-FB-AR2
#DIV/0!
1224-
M29-FB-F1
#DIV/0!
Page 1
-------
Final Wfs.
123
M29-RB-AR2
#DIV/0!
124
M29-RB-F1
#DIV/0!
125
M29-10-AR2
#DIV/0!
126
M29-10-F1
#DIV/0!
127
M29-11-AR2
#D!V/0!
128
M29-11-F1
#DIV/0!
129
M29-12-AR2
#D1V/0!
130
M29-12-F1
#DIV/0!
131
M29-13-I-AR2
#DIV/0!
132
M29-13-I-F1
#DIV/0!
133
M29-13-I-BH Filtrate
134
M29-13-O-AR2
tDIV/0!
135
M29-13-O-F1
ws.uw
#D1V/0!
136
M29-14-I-AR2
#DiV/0!
137
M29-14-I-F1
#DIV/OI
138
M29-14-O-AR2
Wf, »/
WJflg
#DIV/0!
139
M29-14-O-F1
#DIV/0!
140
M29-15-I-AR2
#DIV/0!
141
M29-15-I-F1
#DIV/0!
142
M29-15-O-AR2
#DIV/0!
143
M29-15-O-F1
#DIV/0!
144
M29-FB-I-AR2
#DIV/0!
145
M29-FB-I-F1
#DIV/0!
146
#DIV/0!
Page 2
-------
PACIFIC ENVIRONMENTAL SERVICES, INC.
Project No.
Client
Location
Page
of
Prepared By Date Checked By Date Sheet Title
WLW
•16?
(4o <4?.Z&5
fgp
- r
-------
PACIFIC ENVIRONMENTAL SERVICES, INC.
Location
/o
Page
of
Prepared By Date, Checked By Date Sheet Title
'A'
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.4
.
wr
-------
f, •«, "-.T3-
~?$*3$£
PACIFIC ENVIRONMENTAL SERVICES, INC.
Project No.
Page of
Client
Location
Prepared By
DBAS
Checked By
Date
Sheet Title
- 6
0=4 ...... r
-V- ' ........... -
-------
PACIFIC ENVIRONMENTAL SERVICES. INC.
Method 5 Tare Weights
Central Park West
5001 South Miami Boulevard, P.O. Box 12077
Research Triangle Park, North Carolina 27709-2077
(919) 941-0333 FAX: (919) 941-0234
Project Number: 5401.004
Item Weighed:
Beakers
Date:
Time
R.H {%)
Temp (°F)
Std. Wt. (g)
Analyst
Lab Sample ID No.
101
102
103
104
105
106
107
108
109
110
111
112
113
114
115
116
117
118
119
120
121
122
123
124
125
126
127
128
129
130
131
132
133
134
135
136
137
138
••••
^^^^H
^^^H
^^^H
^^^H
••I^H
Field Sample ID No.
M29-1-A-AR2
M29-1-A-F1
M29-1-B-AR2
M29-1-B-F1
M29-2-A-AR2
M29-2-A-F1
M29-2-B-AR2
M29-2-B-F1
M29-3-A-AR2
M29-3-A-F1
M29-3-B-AR2
M29-3-B-F1
M29-4-AR2
M29-4-F1
M29-5-AR2
M29-5-F1
M29-6-AR2
M29-6-F1
M29-7-AR2
M29-7-F1
M29-FB-AR2
M29-FB-F1
M29-RB-AR2
M29-RB-F1
M29-10-AR2
M29-10-F1
M29-11-AR2
M29-11-F1
M29-12-AR2
M29-12-F1
M29-13-I-AR2
M29-13-I-F1
M29-13-I-BH Filtrate
M29-13-O-AR2
M29-13-O-F1
M29-14-I-AR2
M29-14-I-F1
M29-14-O-AR2
10/31/96
9:30 AM
<50
72.0000
100.0008
MDM
1st
97.7886
102.9615
108.2864
102.0488
105.4286
100.2295
113.8441
98.8095
105.8905
105.1453
102.0304
96.1886
104.7800
105.1476
110.9719
107.7683
112.7266
109.7484
103.9463
101.6254
104.2602
105.6653
103,8623
107.9741
111.6037
107.6316
118.0522
108.7185
105.0986
104.2645
103.7448
114.9331
101.4529
106.6482
104.5788
102.2150
114.2796
101.1084
10/31/96
4:00 PM
100.0018
MDM
2nd
97.7894
102.9625
108.2876
102.0496
105.4297
11/1/96
12:00 PM
99.9999
MDM
3rd
97.7880
102.9608
108.2858
102.0476
105.4277
100.2286
113.8432
98.8089
105.8043
105.1446
102.0299
96.1877
104.7788
105.1464
110.9709
107.7672
112.7255
109.7473
103.9453
101.6255
104.2591
105.6639
103.8612
107.9728
111.3027
107.6304
118.0512
108.7172
105.0976
104.2634
103.4765
114.9323
101.4521
106.6473
104.5779
102.2141
114.2786
101.1075
11/4/96
8:45 AM
99.9999
MDM
4th
97.7871
102.9598
108.2847
102.0466
105.4269
100.2277
113.8421
98.8081
105.8036
105.1436
102.0292
96.1870
104.7782
105.1461
110.9702
107.7666
112.7252
109.7471
103.9451
101.6254
104.2592
105.6642
103.8613
107.9731
111.3021
107.6299
118.0504
108.7167
105.0975
104.2629
103.4767
114.9317
101.4517
106.6468
104.5776
102.2138
114.2785
101.1074
11/4/96
3:15 PM
99.9997
MDM
5th
97.7876
102.9603
108.2852
102.0471
105.4274
100.2283
113.8423
98.8082
105.8036
105.1438
102.0290
96.1868
104.7781
110.9701
107.7663
111.3018
118.0502
114.9311
11/5/96
8:30 AM
99.9998
MDM
6th
100.2287
114.9321
11/5/96
3:30 PM
99.9999
MDM
7th
114.9318
Difference
(mg)
0.5
0,5
0.5
0.5
0.5
0.4
0.2
0.1
0
0.2
0.2
0.2
0.1
0.3
0.1
0.3
0.3
0.2
0.2
0.1
0.1
0.3
0.1
0.3
0.3
0.5
0.2
0.5
0.1
0.5
0.2
0.3
0.4
0.5
0.3
0.3
0.1
0.1
Average
Beaker
Tare Weight
(g)
97.7874
102.9601
108.2850
102.0469
105.4272
100.2285
113.8422
98.8082
105.8036
105.1437
102.0291
96.1869
104.7782
105.1463
110.9702
107.7665
112.7254
109.7472
103.9452
101.6255
104.2592
105.6641
103.8613
107.9730
111.3020
107.6302
118.0503
108.7170
105.0976
104.2632
103.4766
114.9320
101.4519
106.6471
104.5778
102.2140
114.2786
101.1075
Filter No(s).
-
301633-301666
-
301 669-30 1 680-301 655
-
301664-301663
-
301668
-
301670-301677
-
301681
-
301672
-
301665
-
301448
-
301676
-
301576
-
301645-301650-301562
-
301486
-
301679
-
301643
-
301646-301647
-
301654
-
301673-301637
-
Filter
Tare Weight(s]
(mg)
898.9
1346
894.1
445.5
896.9
445.7
445.3
445.4
341.8
444.2
323.7
1217.8
342
457.6
445.3
894.6
445.8
888.5
— — 4 — /
Total
Tare Weight
(9)
97.7874
103.8590
108.2850
103.3929
105.4272
101.1226
113.8422
99.2537
105.8036
106.0406
102.0291
96.6326
104.7782
105.5916
110.9702
108.2119
112.7254
110.0890
103.9452
102.0697
104.2592
105.9878
103.8613
109.1908
111.3020
107.9722
118.0503
109.1746
105.0976
104.7085
103.4766
115.8266
101.4519
106.6471
105.0236
102.2140
115.1671
101.1075
fOp
-------
O PACIFIC ENVIRONMENTAL SERVICES. INC.
Central Park West
5001 South Miami Boulevard, P.O. Box 12077
Research Triangle Park, North Carolina 27709-2077
(919)941-0333 FAX: (919) 941-0234
Method 5 Tare Weights
10/31/96
9:30 AM
<50
72.0000
100.0008
MOM
Lab Sample ID No.
Field Sample ID No.
1st
10/31/96
4:00 PM
100.0018
MDM
2nd
11/1/96
12:00 PM
99.9999
MDM
3rd
11/4/96
8:45 AM
99.9999
MDM
4th
11/4/96
3:15PM
99.9997
MDM
5th
11/5/96
8:30 AM
99.9998
MDM
6th
11/5/96
3:30 PM
99.9999
MDM
7th
Difference
(mg)
Average
Beaker
Tare Weight
(g)
Filter No(s).
Filter
Tare Weight(s)
(mg)
Total
Tare Weight
(g)
139
M29-14-O-F1
115.1488
115.1480
115.1474
115.1469
0.5
115.1472
301648
446.1
115.5933
140
M29-15-I-AR2
116.0181
116.0172
116.0165
116.0160
0.5
116.0163
116.0163
141
M29-15-I-F1
106.7710
106.7704
106.7702
0.2
106.7703
301644-301639
898.7
107.6690
142
98.5001
98.4994
98.4977
98,4970
98.4977
98.4979
0.2
98.4978
98.4978
143
M29-15-O-F1
110.6229
110.6222
110.6217
0.5
110.6220
301624
448.9
111.0709
144
M29-FB-I-AR2
99.6315
99.6307
99.6304
0.3
99.6306
99.6306
145
M29-FB-I-F1
102.3063
102.3056
102.3054
0.2
102.3055
301628
450.6
102.7561
146
100.7800
100.7792
100.7786
100.7782
0.4
100.7784
100.7784
-------
METHOD 5
TARE WEIGHT
Project Number:
'd-Ol ~
Item Weighed:
Itfe
-M-
fc/r^"
7r#r
HEfe
Date
R.H. (%)
Temp. (°F)
Std. Wt.
Analyst
ID Number
Field Sample
Number
1st
2nd
3rd
4th
5th
Final
Wt, (g)
Tare
Wt. (g)
Difference
(mg)
/OJ.
103
62, 646$
IOZ.04M
(06
1 (3.8432-
IdB
no
in
IfZ
IB
104,
«
in.
101,141?
\63.
s
n\
I M 3601-
(05* 66*%
(13
124
(03, 8to
103.
-------
METHOD 5
TARE HEIGHT
Project Humbert
Item Weighedi
PEA*
/ 1
Date
/• /t ft 6
R.H. (%)
Std. Ht.
1(30.0008
Analyst
10 Number
Field Sample
Number
1st
4th
5th
Final
Wt. (g)
Tare
Wt. Cg)
Difference
11,
ff ,3*710
(01.
ffg.asof-
(6
„ m
63&W
(0^
114,3332'
'14-^23
1
lti.6433
SI
167.7(41
4f
1(0.
(16.
102.30
167,
m
'00,
7^ /,
-------
TARED FILTER LOG
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*P1 ste* tic* t>/jE. 35<9.*f
#2^/25 ,orf T/ 330,2,
#3
AVERAGE
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#1Sld! i.rtf 3-3F W/*
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413
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pStt 32S.S
321.3
#4
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DATE/TIME NAME MASS
frf 5
#4.
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332.^5
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331.^
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**' PSM 332,1
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#4.
337.5
#3.
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AVERAGE
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323.$
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DATE/TIME NAME MASS
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•
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•
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.
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•
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#3
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J%r./
5/7-?
AVERAGE -/
-------
• JL*J
b—
TARED FILTER LOG
NO • 20/cfl*) 1 p NO.:
DATE/TIME NAME MASS
#1 A/7/u 0630 &ff y
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TARED FILTER LOG
fsin • to/t>
-------
CASE NARRATIVE
Analysis of Samples for the Presence of Trace Metals
Method 29 April 1996 Rev.
Client:
Pacific Environmental Services
TLI Project Number: 39568
Date: December?, 1996
This report should only be reproduced in full.
Any reproduction of this report requires permission from
Triangle Laboratories, Inc.
Rev, 25-Sep-96
Triangle Laboratories, Inc.
6320 Quadrangle Drive P.O. Box 13485
Suite 240 Research Triangle Park,
Chapel Hill, NC 27514 North Carolina 27709
919-493-0877 Fax # 919-493-1193
\
-------
Triangle Laboratories, Inc. December 7,1996
Case Narrative TLI Project f: 39568
Overview
Nine train samples, a field blank train sample and a reagent blank train sample were
analyzed for arsenic (As), beryllium (Be), cadmium (Cd), cobalt (Co), chromium (Cr),
manganese (Mn), nickel (Ni), lead (Fb), antimony (Sb), selenium (Se), and mercury (Hg).
For all analyses, the samples and associated QC samples were prepared and analyzed
following the guidelines of Method 29 April 1996 Rev. Results reported relate only to
the items tested.
OC Remarks
The release of this set of data by Triangle Laboratories, Inc. was authorized by the Quality
Control Chemist who has reviewed each sample data package individually following a
series of inspections/reviews. When applicable, general deviations from acceptable QC
requirements are identified below and comments are made on the effects of these
deviations upon the validity and reliability of the results. Specific QC issues associated
with this particular project are:
Sample Receipt:
Ten train samples, a field blank train sample and a reagent blank train sample were received
without coolant on November 12-14,1996 in good condition. The filter for sample M29-1-A
was received on November 14,1996 without coolant in good condition under project* 39590
and combined and processed with project # 39568. Sample M29-4 was archived per client's
request.
Sample Preparation:
Laboratory documentation of the sample preparation is included in the data package.
Instrumentation:
Arsenic (As), chromium (Cr), manganese (Mn), nickel (Ni), lead (Pb), antimony (Sb), and
selenium (Se) concentrations were determined by Inductively Coupled Plasma Emission
Spectroscopy (ICP).
Beryllium (Be), cadmium (Cd), and cobalt (Co)concentrations were analyzed by Graphite
Furnace Atomic Absorption (GFAA). Cadmium (Cd), and cobalt (Co)concentrations for
sample M29-1-A, MB2 and LCS2 were analyzed by Inductively Coupled Plasma
Emission Spectroscopy (ICP).
Mercury (Hg) concentrations were determined by Cold Vapor Atomic Absorption
(CVAA).
-------
Triangle Laboratories, Inc. December 7,1996
Case Narrative TLI Project #: 39568
The linear range for the instrument TJA 6 IE Trace Analyzer was based on four standards
and a blank, which established a correlation coefficient value greater than or equal to
0.995. A calibration curve, based on a blank and one standard, is established for each
analytical ran, followed by a check high standard and an initial calibration verification
(ICV). The check high standard does not deviate from the calibration curve by more than
5%. In addition, continuing calibration verifications (CCVs) are performed throughout
the analytical ran.
A Reporting Detection Limit (RDL) is used instead of an Instrument Detection Limit
(IDL). The spectrometer and atomic absorption instruments can achieve low detection
limits between 0.2-8 ppb levels for many analytes. Triangle Labs is using RDL values of
1-10 times the IDL as detection limits for reporting purposes.
Data Review:
All analytes found in the method blank (MB) are detected at a level equal to or less than
the respective Reporting Detection Limits (RDLs).
Some samples were analyzed within the 28 day sampling to analysis holding time for Hg.
Due to the delay in receipt of the samples and the lengthy preparation process, the back
half samples for M29-6, M29-7, M29-3, M29-FB, M29-FB, and the front half samples for
M29-1-B, M29-2-A, M29-2-B, M29-3-A, M29-3-B, M29-5, M29-6, M29-7, M29-FB,
and M29-RB were analyzed outside of holding time. All samples were analyzed within
the six month sampling to analysis holding time for all other requested analytes.
The pre-digestion spike (MS) and the pre-digestion spike duplicate (MSD) for Hg for the
sample M29-6 BH demonstrated percent recoveries outside the QC criteria, which may
indicate significant matrix effects specific to this analytes in the native sample matrix.
Please note that this sample should be considered biased low due to matrix interferences.
The post-digestion spike (PDS) for As, Cr and Sb for the sample M29-1-B demonstrated
percent recoveries outside the QC criteria, which may indicate significant matrix effects
specific to these analytes in the native sample matrix. Please note that this sample should
be considered biased low for these analytes due to matrix interferences.
The recoveries for the post-digestion spike (PDS) for sample M29-1-B are not reporte'd
for Mn, Ni, Pb, and Se. The spike concentrations added were insignificant in comparison
to the levels of these analytes present in the native sample.
A duplicate analysis is not reported for elements analyzed by GFAA. The GFAA
instrument analyzes two separate aliquots of the sample and averages the values for a final
result. These two analyses agree within a RPD of 20% or a second run is done for that
sample. The ICP instrument analyzes one continuous aliquot three times and averages the
values for a final result. The ICP does not take two separate aliquots, therefore a DA is
performed.
-------
Triangle Laboratories, Inc. December 7,1996
Case Narrative TLI Project*: 39568
The serial dilution results for Co, Cr, Ni, Pb, and Se for the sample M29-1-A
demonstrated RPDs outside the QC control criteria of 10,0 percent, which indicates the
presence of a significant amount of interferents specific to these analytes in the native
sample matrix.
Please note that this sample should be considered biased low for these analytes due to
matrix interferences.
QC requirements:
The duplicate analyses for analytes analyzed by TCP cannot be considered valid qualifiers if
the concentrations of the analytes in the original and/or duplicate sample are not at least
ten times the respective RDLs. The RPDs for these analyses are indicated by or "
-------
Triangle Laboratories, Inc. December 7,1996
Case Narrative TLI Project #: 39568
By our interpretation, the analytical data in this project are valid based on the guidelines of
Method 29 April 1996 Rev. Any specific QC concerns or problems have been discussed in
the QC REMARKS section with emphasis on their effect on the data. Should Pacific
Environmental Services have any questions or comments regarding this data package,
please feel free to contact Project Scientist, Selena Armistead, at (919) 544-5729 ext.268.
For Triangle Laboratories, Inc.,
Report Preparation Quality Control
Linda F, Jones
Report Preparation Chemist Report Preparation Chemist
The total number of pages in this data package i
5
-------
/ML
TRIANGLE LABORATORIES, INC.
LIST OF CERTIFICATIONS AND ACCREDITATIONS
FNMRQNMENTAL
American Association for Laboratory Accreditation. Expires July 31, 1997. Certificate
Number 0226-01. Accreditation for technical competence in Environmental Testing.(Including
Waste Water, Sol/Haz Waste, Pulp/Paper, and Air Matrices) Parameters are AOX/TOX, Volatiles,
Pesticides, PCB's, BNA's, and Dioxin/Furan. Method 1613 for Drinking Water.
State of Alabama, Department of Environmental Management Expires December 31, 1997.
Laboratory I.D. #40950. Drinking Water for Dioxin.
State of Alaska, Department of Environmental Conservation. Expires December 31, 1996.
Drinking Water for Dioxin.
State of Arizona, Department of Health Services. Expires May 26, 1997. Certificate 8AZQ423.
Drinking Water for Dioxin, Dioxin in WW and S/H Waste.
State of Arkansas, Department of Pollution Control and Ecology. Expires February 14,
1997. Primary No. 94-06497. Pulp/paper, soil, water, and Hazardous Waste for Dioxin/Furan;
AOX/TOX.
State of California, Department of Health Services. Expires August 31, 1997. Certificate
#1922. Selected Metals in Waste Water; Volatiles, Semi-volatiles, and Dioxin/furan in WW and
Sol/Haz Waste. Dioxin in Drinking Water.
State of Connecticut Department of Health Services. Expires September 30, 1997.
Registration # PH-0117. Dioxin in Drinking Water.
Delaware Health and Social Services. Expires December 31,1996. Certificate #NC 140. Dioxin
in drinking Water.
Florida Department of Health and Rehabilitative Services. Expires June 30, 1997,Dioxin in
DW. Drinking Water ID HRS# 87424. Metals, Extractable Organics (€C/MS), Pesticides/PCB's
(GC) and Volatiles (GC/MS) in Environmental Samples. Environmental water ID HRS* E87411.
Hawaii Department of Health. Expires March 1, 1997. Dioxin in drinking water. "Accepted"
status for regulatory purposes.
R«vissd Novtmbw 19,1996 ipw Triangle Laboratories, Inc.
Printed Nevembw 20,1996 801 Capitols Drive P.O. Box 13485
Durham, NC 277134411 Research Triangle Park, NC 27709-3485
919-544-5729 Fax #919-544-5491 6
-------
Idaho Department of Health and Welfare. Expires November 30, 1997. Dioxin in Drinking
Water.
State of Kansas, Department of Health and Environment Expires January 31, 1997.
Environmental Analyses/Non potable Water and Solid and Hazardous Waste. Method 1613 for
drinking water. ID #s - Drinking water and/or pollution control - E-215. Solid or Hazardous Waste -
E-1209.
Commonwealth of Kentucky, Department for Environmental Protection. Expires December
31,1ii6. ID#900SO. Drinking Water for Dioxin.
Maryland Department of Health and Mental Hygiene. Expires September 30, 1997.
Certification #235. Drinking water by Method 1613A.
State of Michigan, Department of Public Health. Expires March 31, 1997. Drinking water by
Method 1613.
Montana Department of Health and Environmental Services. Expires December 31, 1996.
Dioxin in Drinking Water.
State of New Jersey, Department of Environmental Protection and Energy. Extended by
state. Temporary certificate until June 30, 1997 or sooner. ID #67851. BNAs and Volatiles.
Drinking water for Dioxin. ". -.
State of New Mexico, Environment Department Expires July 31, 1997. Drinking water for
Dioxin.
New York State Department of Health. Expires March 31, 1997. ID #11026. Environmental
Analyses of non-potable Water, Solid and Hazardous Waste. Method 1613 in DW.
State of North Carolina, Department of Environment Health and Natural Resources Expires
December 31,1996. Certificate # 37751. Drinking Water for Dioxin.
State of North Carolina, Department of Environment, Health, and Natural Resources,
Division of Environmental Management Expires December 31, 1997. Certificate # 485.
Metals, pesticides & PCBs, semi-volatiles and volatiles; TCLP.
State of North Carolina, Department of Environment, Health, and Natural Resources •
Division of Radiation Protection. Expires april 30, 1998. General License No. 32-0875-OG;
Specific License No. 0954-1.
Revised November 19,1996 apw
Printed November 20,1996
-------
North Dakota State Department of Health and Consolidated Laboratories. Expires
December 31,1996. Certificate # R-Q76. Effective October 4,1993. Dioxin in Drinking Water,
Oklahoma Department of Environmental Quality. Expires May 31, 1997. Laboratory #9612.
Dioxin by 1613A, 8290 and 8280.
State of South Carolina, Department of Health and Environmental Control. Expires April 1,
1997. Certificate number #99040001 (drinking water). Expires August 31, 1997. Certificate
number #99040002 (other parameters). Dioxin/Furans, BNA, Volatiles, and PCBs/pesticicles
under Clean Water Act, 2,3,7,8-TCDD for Drinking Water, and Organic extractables for Solid and
Hazardous Waste.
State of Tennessee. Department of Environment and Conservation. Expires February 5,
1999.10*02992. Method 1613 Drinking water only.
U.S. Department of Agriculture Soil Permit Expires September 30, 2001. Permit No, S-3790
Revised. Under the authority of the Federal Plant Pest Act, permission is granted to receive
foreign soil samples for use in labatory analysis.
U.S. Army Corps of Engineers. Expires November 30, 1997. Validated to perform methods
8280 & 8290 for Lockboume Landfill Site Investigation, Defense Distribution Depot Projects, and
assorted projects for the USAGE North Pacific Division Laboratory.
U.S. EPA Region V. Expires December 29,1995. Dioxin in Drinking Water.
U.S. EPA Region VIII, for the State of Wyoming. Expires November 13, 1997. Dioxin in
Drinking Water.
State of Utah, Department of Health. Expires December 31, 1997. Certificate Number E-166.
Certification for the following parameters: Semi-Volatiles and Volatiles under RCRA; Volatiles
under Clean Water Act; Dioxin/furans by Method 8280; Drinking water for Dioxin by Method 1613;
Metals including Mercury and Microwave Digestion.
Commonwealth of Virginia, Department of General Services, Division of Consolidated
Laboratory Services. Expires June 30,1997. ID # 00341. Dioxin in Drinking Water.
State of Washington, Department of Ecology. Expires September 11, 1997. Lab Accreditation
Number C067. Scope of Accreditation applies to water analyses for Poiychlorinated Dibenzo-p~
dloxins and Poiychlorinated Dibenzofurans, BNA Extr (Semivolatile) Organics and Purgeable
(Volatile) Organics.
State of Washington, Department of Health. Expires April 30,1997. Drinking water for Dioxin.
Revised November 19,1996 apw
Printed November 20,1996
8
-------
State of West Virginia, Department of Health. Expires December 31, 1996. Certificate No.
9923(C). Drinking water for Dioxin.
State of Wisconsin, Department of Natural Resources. Expires June 30, 1997. Laboratory ID
Number 999869530. Certification for the following categories of Organics: Purgeable,
Base/Neutral, Acid, PCBs, and Dioxin.
PHARMACEUTICAL
Drug Enforcement Agency (DEA). Expires November 30, 1997. Registration number
RT01195835. Controlled substance registration for schedules 1,2,3,3N,4,5.
N.C. Department of Human Resources, Expires October 31, 1997. Registration number NC-
PT 0000 0031. North Carolina controlled substances registration. Application submitted for
renewal.
Food & Drug Administration (FDA) Registration, Expires July 1997, ID #s 001500 1053481.
Annual registration of drug establishment Annual registration of drug establishment.
OTHER
Clinical Laboratory Improvement Amendments (CLIA) Registration. Expires May 30, 1997.
ID # 34D0705123. Department of Health & Human Services, Health Care Financing
Administration.
•»
U.S. EPA Large Quantity Hazardous Waste Generator. No expiration date. EPA ID
#NCD982156879. Permit indicates that the laboratory is a large generator of hazardous waste.
North Carolina Radioactive Materials License. Expires April 30 1998. License No. 032-0954-
1. License authorizes the licensee to receive, acquire, own, possess, transfer, import and use
such radioactive materials as designated.
North Carolina General License for Radiation Protection. No. expiration date. License No.
032-875-OG. The general license applies only to radioactive material contained in devices which
have been manufactured and labeled in accordance with specific requirements.
Revised November 19,1996 apw
Printed November 20,1996
-------
ABBREVIATIONS
BackHaif
CCB = Continuing Calibration Blank
CCV = Continuing Calibration Verification
CHECK HS = Check High Standard
D - DUP « Analytical Duplicate (Prepared Duplicate)
DA = Duplicate Analysis
FH « Front Half
FV = Hnal Digestate Volume
ICB = Initial Calibration Blank
ICV ss Initial Calibration Verification
ICSAB «Interference Check Solution (Solution AB)
1 = Tnirial
F = Final
Solution AB contains common interferents in addition to the onalyte of interest,
DDL = Instrument Detection T-irm'r
L - Serial Dilution
LCS = Laboratory Control Strike Samcle
* 4, «,
MB = Method Blank
MPV = Mercury Preparation Volume
MS = Pre-digestion Spike
MSD = Pre-digestion Spike Duplkate
N/A = Not Applicable
N/Av = Not Available
y/V = Not Valid
PDS = Post-digestion Spike
%REC = Percent Recovery
RDL = Reporting Detection Limit
RPD = Relative Percent Difference
T = Analytical Triplicate (Prepared Triplicate; for Hg analysis by Method 7471 only)
TV = Total Sample Volume
< = Analyte concentration in the sample is less than the respective RDL
10
-------
STANDARD CONCENTRATIONS
for the TJA 61E TRACE ANALYZER
Analvte
As
B
Be
Cd
Co
Cu
K
Ms
Mo
Ni
Pb
Se
Sr
TI
Zn
Units
ppb
fiiiiB
PPb
PPb
ppb
ppb
PPb
ppb
HighStd
1000
1000
1000
1000
1000
1000
ICV/CCY
500
500
500
500
500
ICSAB
500
500
500
500
500
500
500
10000
5000
ppb I 1000
PPb
PPb
PPb
ppb
ppb
Ppb
1000
1000
1000
1000
1000
1000
1000
19000
500
500000
500
500
500
500
500
500
500
500
500
500
500
650
500
500
RDL
220
30
1
12
Wavelength
1890
2496
3130
2265
2286
3247
7664
2790
2020
2316
2203
1960
4215
1908
2062
Note: Use this reference page to review the raw data from the TJA 6 IE Trace Analyzer.
This page includes the standard concentrations for the check high standard, initial calibration
verification (ICV)t continuing calibration verification (CCV), and the interference check solution
(ICSAB). In addition the reporting detection limit (RDL) and wavelength are reported for each
analyte.
Revision Date: 15-M-96
1 1
-------
CALCULATIONS FOR MULTI-METALS TRAIN SAMPLES
RESULTS FOR TRACE METALS (except mercurr):
RESULT in (ig (Front Half) = ug/L * ml FV * DF
1000
RESULT in jig (Back Half & Impingers) = fig/L*(mlTV/mlused^*mlFV*DF
1000
/ <** i ' { C\ 8 f\ \
ml FV ss final volume in ml v
ml TV = total volume in ml
DF = Dilution Factor
RESULT in ^g for the combined Front Half & Back Half samples have the same calculation as the
Back Half & Impinger samples.
RESULTS FOR MERCURY (He);
RESULT in ug (Front Half) = ug/L * (ml FV/ml aliquot) * MPV * DF
RESULT in ug (Back Half & Impingers) = ug/L * (ml TV/ml aliquot) * MPV * DF
MPV (mercury preparation volume) = 0. 1 L or 0.008 L
ml TV = total volume in ml
DF = Dilution Factor
%REC (Percent Recovery) for MS/MSP and He spikes:
%REC = Spike sample results - original sample results * 100
true spike sample results
%REC (Percent Recovery) for PDS;
%REC = Spike sample itg/L cone. - original sample fig£L cone. * 100
spike cone. (jig/L)
%REC (Percent Recovery) for LCS/LCSD;
%REC = Spike sample ug/L cone. * 100
spike cone. (jig/L)
RPDs;
loco
RPD= I Result2-Result 1 I * 100
(Result 2-f Result l)/2
12
-------
Client: Pacific Environmental Services
Project Number: 39568
Sample Report
Client Sample ID:
TLI Sample ID:
Date Received:
Date Prepared:
Date Analvzed:
Matrix:
M29-1-A
146-4.26-1ABC
November 12-14. 1996
November 18-25, 1996
Nov. 22-26 & Dec,2-4. 1996
Air
As
Be
Cd
Co
Cr
Mn
Ni
Pb
Sb
Se
50.019
4.160
20.698
209.308
306.734
427.861
523.099
404.493
128.116
1058.346
990
990
990
990
990
990
990
990
990
990
540
540
540
540
540
540
540
540
540
540
iilHiilii
100
100
100
100
100
100
100
100
100
100
1
50
1
1
1
1
1
1
1
1
illiii!:iilP:::-:;
9.17
38.1
3,79
38.4
56.2
78.4
95.9
74.2
23.5
194
•*
. ifc
Triangle Laboratories, Inc.
801 Capitola Drive * Durham, North Carolina 27713
Tele: (919) 544-5729 * Fax: (919) 544-5491
Printed: 07-Dec-96 at 03:53 PM
13
-------
Client: Pacific Environmental Services
Project Number: 39568
Sample Report
Client Sample ID:
TLI Samole ID:
Date Received:
Date Prepared:
Date Analyzed:
Matrix:
M29-1-AL
1464.26-1ABCL
November 12-14. 1996
November 18-25. 1996
Nov. 22-26 & Dec.2-4. 1996
Air
lllliililHill
As
Be
Cd
Co
Cr
Mn
Ni
Pb
Sb
Se
U> 12.738
€ 0.830
<" 4.544
7.< 48.961
1° 83.791
•w 92.844
3» 122.376
*e 99.337
t° 29.393
*o 253.483
T 990
t 990
I 990
IX 990
t 990
1 990
J 990
r 990
f 990
3 990
540
540
540
540
540
540
540
540
540
540
Ulliiiiilt
100
100
100
100
100
100
100
100
100
100
liiliWii
lliliilii
5
250
5
5
5
5
5
5
5
5
Illliil:^;':1"' .
ilUMlF .•'-••.,
11.7
< 45.8
4.17
44.9
76.8
85.1
112
91.1
26.9
232
•-
\CP
,cp
Itp
l^f
.op
lip
Triangle Laboratories, Inc.
801 Capitoia Drive * Durham, North Carolina 27713
Tele: (919) 544-5729 * Fax: (919) 544-5491
Printed: 07-Dec-96 at 03:53 PM
14
-------
Client: Padfic Environmental Services
Project Number: 39568
Sample Report
Client Sample ID:
TLI Sample ID:
Date Received'
Date Prepared:
Date Analyze^:
Matrix:
M29-1-B
146-4-2ABCD
November 12-14. 1996
November 18-25, 1996
Nov. 22-26 & Dec.2-4, 1996
Air
liiiiiiiliB
As
Be
Cd
Co
Cr
Mn
Ni
Pb
Sb
Se
41.054
1.210
5.400
8.000
211.504
246.464
435.924
387.141
100.317
1266.043
1098
1098
1098
1098
1098
1098
1098
1098
1098
1098
613
613
613
613
613
613
613
613
613
613
:-:-£--.-:•:- -. ;• -:-:g;^4-:vvv::.'':>v'-
100
100
100
100
100
100
100
100
100
100
liiimiii
1
250
10
50
1
1
1
1
1
1
llllilili;!'":^-:
ililllip'':.;v;;
7.35
54.2
9,67
71.6
37.9
44.1
78.1
69.3
18.0
227
•-
Triangle Laboratories, Inc.
801 Capitola Drive * Durham, North Carolina 27713
Tele: (919) 544-5729 * Fax: (919) 544-5491
Printed: 07-Dec-96 at 03:53PM
15
-------
Client: Pacific Environmental Services
Protect Number: 39568
Sample Report
Client Sample ED:
TL! Sample ID:
Date Received:
Date Prepared:
Date Analyzed*
Matrix:
M29-2-A
146-4-3ABCDE
November 12-14 1996
November 18-25, 1996
Nov. 22-26 & Dec.2-4. 1996
Air
As
Be
Cd
Co
Cr
Mn
Ni
Pb
Sb
Se
42.748
8.690
5.500
16.000
305.982
1129.541
486.575
896.686
98.221
600.025
1110
1110
1110
1110
1110
1110
1110
1110
1110
1110
"-X'l'X-X-K-X-X-kX-'-X-"-"-:-'-"-'-"-"
630
630
630
630
630
630
630
630
630
630
100
100
100
100
100
100
100
100
100
100
:-:-:-:vX*ii4:%j*:vi;4':-""''" '-"•••"•
iiilliiieip*;
llliiiiilll
1
50
20
20
1
1
1
1
1
1
iPiMfef--"
7.53
76.6
19.4
56.4
53.9
199
85.7
158
17.3
106
-
Triangle Laboratories, Inc.
801 Capitola Drive * Durham, North Carolina 27713
Tele: (919) 544-5729 * Fax: (919) 544-5491
Printed: 07-Dec-96 at 03:53 PM
16
-------
Client; Pacific Environmental Services
Protect Number: 39568
Sample Report
Client Sample ID:
TLI Sample ID:
Date Received:
Date Prepared:
Date Analyzed:
Matrix:
M29-2-ADA
1464-3ABCDEDA
November 12-14. 1996
November 18-25. 1996
Nov. 22-26 & Dec.2-4. 1996
Air
liiliiiiftii
As
Be
Cd
Co
Cr
Mn
Ni
Pb
Sb
Se
42.760
N/A
N/A
N/A
308.336
1136,623
489.815
906.651
101.329
603.221
1110
1110
1110
1110
1110
1110
1110
1110
1110
1110
S^^SgsSPSBBS*
^lliilliilli
630
630
630
630
630
630
630
630
630
630
100
100
100
100
100
100
100
100
100
100
llliiiiiill
1
1
1
1
1
1
1
1
1
1
iiJjjj$j$jjL .'.;.; i
llilillilli,.:::;;
7.53
N/A
N/A
N/A
54.3
200
86.3
160
17.9
106
*-
Triangle Laboratories, Inc.
801 Capitola Drive * Durham, North Carolina 27713
Tele: (919) 544-5729 * Fax: (919) 544-5491
Printed: 07-Dec-96 at 03:53 PM
-------
Client: Pacific Environmental Services
Protect Numben 39568
Sample Report
Client Sample ID:
TLI Sample ID:
Date Received:
Date Prepared:
Date Analyzed:
Matrix:
M29-2-B
146-4-4ABCD
November 12-14. 1996
November 18-25. 1996
Nov. 22-26 & Dec.2-4. 1996
Ak
As
32.427
755
415
100
1
5.90
Be
5.150
755
415
100
50
46.8
Cd
7.300
755
415
100
10
13.3
Co
24.800
755
415
100
10
46,1
Cr
260.044
755
415
100
47.3
Mn
955.681
755
415
100
174
Ni
417.723
755
415
100
76.0
Pb
817.664
755
415
100
149
Sb
91.677
755
415
100
16.7
Se
605.787
755
415
100
110
Triangle Laboratories, Inc.
801 Capitola Drive * Durham, North Carolina 27713
Tele: (919) 544-5729 * Fax: (919) 544-5491
Printed: 07-Dec-96 at 03:53 PM
13
-------
Client: Pacific Environmental Services
Protect Number: 39568
Sample Report
Client Sample ID:
TLI Sample ID:
Date Received:
Date Prepared:
Date Analyzed:
Matrix:
M29-3-A
146-4-5ABCD
November 12-14 1996
November 18-25. 1996
Nov 22-26 & Dec.2-4. 1996
Air
As
Be
Cd
Co
Cr
Mn
Ni
Pb
Sb
Se
:j*ȣglplli
.^^SSBwsM^
iiiiiliiiiii
27.075
7.170
6.600
36.100
158.149
431.660
385.391
252.099
64.504
420.108
iiiiili^^iiiiiiiii
1040
1040
1040
1040
1040
1040
1040
1040
1040
1040
fllllilllSllI
590
590
590
590
590
590
590
590
590
590
llHiiiiii
100
100
100
100
100
100
100
100
100
100
1
50
5
10
1
1
1
1
1
1
Illipil^liC
4.77
63.2
5.82
63.6
27.9
76.1
67.9
44.4
11.4
74.1
*.
Triangle Laboratories, Inc.
801 Capitola Drive * Durham, North Carolina 27713
Tele: (919) 544-5729 * Fax: (919) 544-5491
Printed: 07-Dec-96 at 03:53 PM
-------
Client: Pacific Environmental Services
Project Number: 39568
Sample Report
Client Sample ID:
TLI Sample ID:
Date Received:
Date Prepared:
Date Analyzed:
Matrix:
M29-3-B
146-4-6ABCD
November 12-14. 1996
November 18-25, 1996
Nov. 22-26 & Dec.2-4. 1996
Air
As
Be
Cd
Co
Cr
Mn
Ni
Pb
Sb
Se
19.547
6.380
5.200
31.100
132.546
403.475
357.280
258.304
59.085
479.307
952
952
952
952
952
952
952
952
952
952
ZwiiVttZ&mxXHV
522
522
522
522
522
522
522
522
522
522
>:~¥:S4:*ii&:¥x¥:¥x¥S
100
100
100
100
100
100
100
100
100
100
:-X':;:':-:::'fiiii-:-;:::::i:::-::x::::::::;:::-:'
;«ila^t«x-:
1
50
5
10
1
1
1
1
1
1
wm&m>:'-- \
3.56
58.2
4.74
56.7
24.2
• 73.6
65.2
47.1
10.8
87.4
•-
Triangle Laboratories, Inc.
801 Capiiola Drive * Durham, North Carolina 27713
Tele: (919) 544-5729 * Fax: (919) 544-5491
Printed: 07-Dec-96 at 03:53 PM
20
-------
Client: Pacific Environmental Services
Project Number: 39S68 ^_____
Sample Report
Client Sample ID:
TLI Sample ID:
Date Received'
Date Prepared:
Date Analyzed:
Matrix:
M29-5
146-4-8ABCDE
November 12-14, 1996
November 18-25. 1996
Nov. 22-26 4 Dec.2-4. 1996
Air
iillttiill
As
25.408
1960
1010
100
1
4,93
Be
0.120
1960
1010
100
0.194
Cd
7.500
1960
1010
100
1.46
Co
46.100
1960
1010
100
8.95
Cr
198.109
1960
1010
100
38.4
Mn
242.497
1960
1010
100
47.1
Ni
136.209
1960
1010
100
26.4
Pb
33.709
1960
1010
100
6.54
Sb
100.991
1960
1010
100
19.6
Se
96.710
1960
1010
100
18.8
Triangle Laboratories, Inc.
801 Capitola Drive * Durham, North Carolina 27713
Tele: (919) 544-5729 * Fax: (919) 544-5491
Printed: 07-Dec-96 at 03:53 PM
21
-------
Client: Pacific Environmental Services
Project Number; 39568
Sample Report
Client Sample ID:
TLI Sample ID:
DajeJSeceived:
Date Prepared:
Date Analyzed:
Matrix:
M29-6
146-4-9ABCDE
November 12-14. 1996
November 18-25. 1996
Nov. 22-26 & Dec,2-4. 1996
Air
ArtaM& i
As
Be
Cd
Co
Cr
Mn
Ni
Pb
Sb
Se
OOTia
fcoto
14.502
0.390
5.400
39.800
171.736
150.871
59.754
51.735
26.884
23.416
•ml. ' \
T&afVbt. i
1724
1724
1724
1724
1724
1724
1724
1724
1724
1724
•luL
Used
909
909
909
909
909
909
909
909
909
909
*fL
Final V<&,
100
100
100
100
100
100
100
100
100
100
O&rttori
Factor
1
1
1
1
1
1
1
1
1
1
Total ug
Result
2.75
< 0.190
1.02
7.55
32.6
28.6
11.3
9.81
5.10
4.44
•-
Triangle Laboratories, Inc.
801 Capitola Drive * Durham, North Carolina 27713
Tele: (919) 544-5729 * Fax: (919) 544-5491
Printed: 07-Dee-96 at 03:53 PM
22
-------
Client: Pacific Environmental Services
Project Number: 39568
Sample Report
Client Sample ID:
TLI Samole ID:
Dat? Received:
Date Prepared:
Date Analyzed:
Matrix:
M29-7-PT
146-4-10ABCDE '
November 12-14. 1996
November 18-25. 1996
Nov. 22-26 & Dec. 2-4
Air
111:1 i — nrnimin 1
*38S&8X:-«m
As
6.995
1900
1000
100
1.33
Be
0.110
1900
1000
100
0.190
Cd
6.000
1900
1000
100
1.14
Co
22.700
1900
1000
100
4.31
Cr
100.899
1900
1000
100
19.2
Mn
99.689
1900
1000
100
18.9
Ni
103.859
1900
1000
100
19.7
Pb
45.854
1900
1000
100
8.71
Sb
43.536
1900
1000
100
8.27
Se
42.654
1900
1000
100
8.10
Triangle Laboratories, Inc.
801 Capitola Drive * Durham, North Carolina 27713
Tele: (919) 544-5729 * Fax: (919) 544-5491
Printed: 07-Dec-96 at 03:52PM
23
-------
Client: Pacific Environmental Services
Project Number: 39568
Sample Report
Client Sample ID:
TLI Sample ID:
Date Received:
Date Prewired:
Date Analvzed:
Matrix:
M29-FB-F1
146-4-11 ABODE
November 12-14. 1996
November 18-25. 1996
Nov. 22-26 & Dec. 2-4
Air
'
As
2.239
228
228
100
0.500
Be
0.120
228
228
100
0.100
Cd
3.800
228
228
100
0.380
Co
1.700
228
228
100
0.170
Cr
63.117
228
228
100
6.31
Mn
49.524
228
228
100
4.95
Ni
32.639
228
228
100
3.26
Pb
13.731
228
228
100
1.37
Sb
27.893
228
228
100
2.79
Se
21.423
228
228
100
2.14
Triangle Laboratories, Inc.
801 Capitola Drive * Durham, North Carolina 27713
Tele: (919) 544-5729 * Fax: (919) 544-5491
Printed: 07-Dec-96 at 03:52 PM
-------
Client: Pacific Environmental Services
Project Number: 39568
Sample Report
Client Sample ID:
TLI Sample ID;
Date Received:
Date Prepared:
Dafe Analvzed:
Matrix:
M29-RB-F1
(\K)
146-4-12ABCE % — /
November 12-14. 1996
November 18-25. 1996
Nov. 22-26 & Dec. 2-4
Air
?'^
r^
As
Be
Cd
Co
Cr
Mn
Ni
Pb
Sb
Se
•mmt$f8&$tm&
12.353
0.120
4.300
4.900
146.993
13.774
86.953
22.424
73.543
68.215
400
400
400
400
400
400
400
400
400
400
400
400
400
400
400
400
400
400
400
400
100
100
100
100
100
100
100
100
100
100
1
1
1
1
1
1
1
1
1
1
iiiiii^iiiiiiii
1.24
< 0.100
0.430
0.490
14.7
1.38
8.70
2.24
. 7.35
6.82
•-
Triangle Laboratories, Inc.
801 Capitola Drive * Durham, North Carolina 27713
Tele: (919) 544-5729 * Fax: (919) 544-5491
Printed: 07-Dee-96 at 03:52PM
-------
Client: Pacific Environmental Services
Project Number: 39568
Sample Report
Client Sample ID:
TLI Sample ID:
Date Received:
Date Prepared:
Date Analyzed:
Matrix:
M29-RB
x. Jf
146-4-12D " '
November 12-14. 1996
November 18-25. 1996
Nov. 22-26 & Dec. 2-4
Air
As
Be
Cd
Co
Cr
Mn
Hi
Pb
Sb
Se
-4.916
0.020
0.100
-0.400
3.921
13.990
-2.322
9.834
8.829
-0.269
70
70
70
70
70
70
70
70
70
70
70
70
70
70
70
70
70
70
70
70
100
100
100
100
100
100
100
100
100
100
y;^g?BE!!agy&m
1
1
1
1
1
1
1
1
1
1
i^i|iiill;f";
IlliSillP^
< 0.500
< 0.100
< 0.100
< 0.150
0.392
1.40
< 0.300
0.983
0.883
< 0.300
••
Triangle Laboratories, Inc.
§01 Capitola Drive * Durham, North Carolina 27713
Tele: (919) 544-5729 * Fax: (919) 544-5491
Printed: 07-Dec-96 at 03:52 PM
-------
Client: Pacific Environmental Services
Protect Number: 39568
QA: Serial Dilution
Client Sample ID:
TLI Sample ID:
Date Prepared:
Date Analyzed:
Matrix:
M29-1-A
146-4.26-1ABC
November 18-25, 1996
Nov. 22-26 & Dec.2-4. 1996
Air
M29-1-AL
I46-4.26-1ABC L
November 18-25. 1996
Nov. 22-26 & Dec.2-4. 1996
Air
V&»ZXii&&i&-»XWHSPS&S:
As
Be
Cd
Co
Cr
Mn
Ni
Pb
Sb
Se
Native Sample
<£XV:X£>>>
50.019
4.160
20.698
209.308
306.734
427.861
523.099
404.493
128.116
1058.346
Serial Dilution
;::<^:<>^:%^
11.7
< 45.8
4.17
44.9
76.8
85.1
112
91.1
26.9
232
xX*XvXvX-:w:\v*Xw:wXw.v
12.738
' 0.830
1 4.544
!•-' 48.961
^ 83.791
* 92.844
3 122.376
v 99.337
•1 29.393
\ 253.483
• .
':-:•: vX-:w;j*spt:-: '•:-:•:
-------
Client: Pacific Environmental Services
Proieet Number: 39568
QA: Duplicate
Client Sample ID:
TLI Sample ID:
Date Prepared:
Date Analyzed:
Matrix'
M29-2-A
146-4-3ABCDE
November 18-25. 1996
Nov. 22-26 & Dec.2-4. 1996
Air
M29-2-ADA
146-4-3ABCDEDA
November 18-25. 1996
Nov. 22-26 & Dec.2-4. 1996
Air
Samle
Dulicate
life-
As
7.53
42.749
7.53
42.760
-------
f
R.-fo
21,11-
M.f-f
24 21-
Z2.6J
Z^. "i^
l.fll*-
*liiiii^^l^
^
Illil^iii:
SBSSgvSSx:::;::x;v::
—
._
—
._
._
Triangle Laboratories, toe.
801 Capitola Drive * Durham, NC 27713
Tele: (919) 544-5729 * Fax: (919) 544-5491
Printed: 07-Dec-96
at
03:51 PM
-------
Client: Pacific Environmental Services
Protect Number. 39568
QA: Method Blank
TLI Sample ID:
Date Prepared:
Date Analyzed:
Matrix:
39568 MB
November 18-25, 1996
Nov. 22-26 & Dee.2-4, 1996
N/A
As
Be
Cd
Co
Cr
Mn
Ni
Pb
Sb
Se
Method Blank
-2.37
0.01
0.00
0.00
-0.02
0.49
-1.26
-0.40
2.02
-3.06
1.5
Pass
Pass
Pass
Pass
Pass
Pass
Pass
Pass
Pass
Pass
Triangle Laboratories, Inc.
801 Capitola Drive * Durham, NC 2771
Tele: (919) 544-5729 * Fax: (919) 544-5491
Printed: 06-Dec-96
at
10:16PM
-------
Client: Pacific Environmental Services
Project Number: 39568
QA: Method Blank
TLI Sample ID:
Date Prepared:
Date Analyzed:
Matrix:
39568 MB2
November 18-25, 1996
Nov. 22-26 & Dec. 2-4
N/A
Be
Cd
Co
Cr
Mn
Ni
Pb
Sb
Se
Method Blank
-2.62
0.04
-0.67
-0.83
-0.06
0.94
-2.70
0.76
0.40
-0.26
1.5
Pass
Pass
Pass
Pass
Pass
Pass
Pass
Pass
Pass
Pass
Triangle Laboratories, Inc.
801 Capitola Drive * Durham, NC 2771
Tele: (919) 544-5729 * Fax: (919) 544-5491
Printed: 06-Dec-96
at
09:41 PM
31
-------
Client: Pacific Environmental Services
Protect Number: 39568
QA: Lab Control Spikes
TLI Sample ID:
Date Prepared:
Date Analyzed:
Matrix:
39568 LCS
November 18-25. 1996
Nov. 22-26 & Dee,2-*. 1996
N/A
Lab Control Spike
Lab Control Spike Duplicate
RPD
Ffecoveiy
As
44.59
50
89%
—
Be
53.90
50
108°/t
Cd
49,00
50
98°/<
Co
42.00
50
84°/c
Cr
47.89
50
96°/<
Mn
48.29
50
97°/<
Ni
46.95
50
94°/<
Pb
46.99
50
94°/<
Sb
48.77
50
98°/<
Se
43.95
50
88°/<
Triangle Laboratories, Inc.
801 Capitola Drive * Duiham, NC 27713
Tele: (919) 544-5729 * Fax: (919) 544-5491
Printed: 06-Dec-96
at.
10:16PM
32
-------
Client: Pacific Environmental Services
Project Number: 39568
QA: Lab Control Spikes
TLI Sample ID:
Date Prepared:
Date Analyzed:
Matrix:
39568 LCS2
November 18-25, 1996
Nov. 22-26 & Dec. 2-4
N/A
mmmmmm
As
Be
Cd
Co
Cr
Mn
Ni
Pb
Sb
Se
Lab Control Spike
S5S¥WW:::»S>Sj?¥i:^£83:
46.22
50.50
46.68
47.15
47.88
47.68
45.63
48.04
49.21
45.07
liiifcii^l
50
50
50
50
50
50
50
50
50
50
92%
101%
93%
94%
96%
95%
91%
96%
98%
90%
Lab Control Spike Duplicate
ilSiiiiiliiil:
^SSJSSfiSSiiSB^JSSSSS
3>K3!f:-;;jMK::W::--<
,
PlfP
—
—
—
—
—
—
—
—
—
—
—
—
—
—
...
—
—
—
—
—
—
—
—
—
—
—
—
—
—
—
—
Triangle Laboratories, Inc.
801 Capitola Drive * Durham, NC 27713
Tele: (919) 544-5729 * Fax: (919) 544-5491
Printed: 06-Dec-96
at
10:16PM
33
-------
Client:
Project Numben
Pacific Environmental Services
39568
Sample Report
Page 1 of 6
Date Received:
Date Pretiared:
p^g Analvwf!:
PATA FTLF.-
Matrix:
November 12-14. 1996
November 18-25, 1996
November 21-26. 1996
AB642. AB643 A; AB644
Air
ANALYTE: Ha
ua/L RDL 0.2
Analvsis Method:
29
Instiumant P E Zeeman 51OO
Spike Cone.
-------
'
Client:
Project Numbers
Pacific Environmental Services
39568
Sample Report
Page 2 of 6
Date Received:
Date Prepared:
Dfitfi Ana^v^£(i'
DATA FILE:
Matrix:
November 12-14. 1996
November 18-25. 1996
November 21-26. 1996
AR642. AB643 & AB644
Air
ANALYTE: Ha
ual RDL- 0.2
Analysis Method:
29
Inshument- P F 7ag{j]an 5100
Spike ft>ne. futfl-^
S
CVAA ANALYTE SUMMARY REPORT
M29-2-B FH
M29-2-B FH D
M29-2-B BH
M29-2-B BH D
M29-2-B HNO3
M29-2-B HN03 D
M29-2-B KMnO4
M29-2-B KMnO4 D
M29-2-B HO
M29-2-B HCI D
M29-3-AFH
M29-3-A FH D
M29-3-ABH
M29-3-A BH D
M29-3-A HNO3
M29-3-AHNO3D
M29-3-A KMnO4
M29-3-A KMnO4 D
M29-3-AHO
M2M-A HCI D
M29-3-B FH
M29-3-B FH D
M29-3-8BH
M29-3-BBHD
M29-3-B HN03
M29^3-B HNO3 D
M29-3-B KMnO4
M29-3-B KMnO4 D
M29-3-BHCI
M29-3-BHCID
146-4-4ABC
146-4-4ABCD
1464-4D
146-4-4DD
14&4-4E
146-4-4ED
146-4-4F
146-4-4FD
14&4-4G
146-4-4GD
146-4-5ABC
146-4-5ABC D
14&4-5D
146-4-5DD
14&4-5E
14&4-5ED
14&4-5F
1464-5FD
14&4-5G
146-4-5GD
146-4-6ABC
14&4-6ABCD
146-4-6D
148-4-6DD
146-4-6E
146-4-6ED
14&4-6F
146-4-6FD
146-1-6G
146^t-6QD
li^Sl
1.415
1.387
0.260
0.263
0.098
0.088
0.192
0.153
0,026
0.075
-0.011
-0.014
0.197
0.194
0.286
0.254
0.822
0.851
0.062
0.072
-0.014
-0.025
0.170
0.159
0.163
0.150
.0.918
0.938
0.078
0.068
ip!
N/A
N/A
680
680
99
99
380
380
235
235
N/A
N/A
900
900
117
117
380
380
232
232
N/A
N/A
860
860
89
89
370
370
22S
228
100
100
N/A
N/A
N/A
N/A
N/A
N/A
N/A
N/A
100
100
N/A
N/A
N/A
N/A
N/A
N/A
N/A
N/A
100
100
N/A
N/A
N/A
N/A
N/A
N/A
N/A
N/A
Hii8i
5
5
5
5
5
5
5
5
5
5
5
5
5
5
5
5
5
5
5
5
5
5
5
5
5
5
5
5
5
5
Hi
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
2.83
2.77
3.54
3.58
< 0.396
< 0.396
< 1.52
< 1.52
< 0.940
< 0.940
< 0.400
< 0.400
< 3.60
< 3.60
0.669
0.594
6.25
6.47
< 0.928
< 0.928
< 0.400
< 0.400
< 3.44
< 3.44
< 0.356
< 0.356
6.79
6.94
< 0.912
< 0.912
2.80
3.56
< 0.396
< 1.52
< 0.940
< 0.400
< 3.60
0,632
6.36
< 0.928
< 0,400
< 3.44
< 0.356
6.87
< 0.912
-
-
-
„
_
-
„
_
_
-
-
-
_
-
•IIP
_
_
_
-
_
--
_
».
»
-
„
-
„
_
-
35
-------
Client:
Project Number:
Pacific Environmental Services
39568
Sample Report
Dale Received:
Date Prepared:
Dfttfi Ana^vze(k
DATA FTIJE:
Matrix:
November 12-14, 1996
November 18-25, 1996
November 21-26. 1996
AB642. AB643 A AB644
Air
Page 3 of 6
ANALYTC: Ha
ua/L RDL 0.2
Anahrsis Method-
29
Instalment* P P Tapn^pn 5100
Spp
-------
Client:
Project Number:
Pacific Environmental Services
39568
Sample Report
Page 4 of 4
Date Received:
Date Prepared:
Date Analyzed:
DAT A FILE:
Matrix:
November 12-14, 1996
November 18-25, 1996
November 21-26,, 1996
A8642. AB643 ft A£644
Air
ANALYTE: Ha
uq/l RDL 0.2
Analysis Method:
29
Instrument P E 7eeman 5100
Spike Gone. Ajg/L)
5
CVAA ANALYTE SUMMARY RETORT
M29-FIELD BUNK FH
M29-RELD BUNK FH D
M29-FIELDBUNKBH
M29-FIELDBUNKBHD
M29-FIELDBUNKHN03
M29-FIELDBUNKHN03D
M29-FIELD BUNK KMnO4
M29-FIELD BLANK KMnO4 D
M29-FIELD BUNK Ha
M29-FIELD BUNK HCI D
M29-HEAGENT BUNK FH
M29-REAGENT BUNK FH D
M29-REAGENT BUNK BH
M29-REAGENT BUNK BH D
M29-REAGENT BUNK HNO3
M29-REAGENT BUNK HNO3 D
M29-REAGENT BUNK KMnO4
M29-REAGENT BLANK KMnO4 D
M29-REAGENT BUNK HCI
M29-REAGENT BUNK HCI D
Dl Water
Dl Water D
146-4-11 ABC
146-4-11 ABC D
146-4-1 1DE
146-4-11DED
146-4-11 E
146*4-11 ED
146-4-1 1F
146-4-1 1FD
146-4-1 1G
146-4-1 1GD
146-4-12ABC
146-4-12ABC D
146-4-12EC
146-4-12EC D
146-4-12C
1 46-4-1 2C D
146-4-12FD
146-4-12FD D
146-4-12GF
146-4-12GFD
146-4-12D
14&4-12D D
-0,025
-0.025
-0.031
-0.037
0.006
0.000
0.003
0.000
-0,003
-0.003
-0.023
-0,028
•0.039
-0.034
0.031
0.022
-0.039
-0.042
0.003
-0.042
-0.025
-0.042
•
N/A
N/A
150
150
52
52
380
380
240
240
N/A
N/A
300
300
100
100
400
400
230
230
70
70
•P
100
100
N/A
N/A
N/A
N/A
N/A
N/A
N/A
N/A
100
100
N/A
N/A
N/A
N/A
N/A
N/A
N/A
N/A
N/A
N/A
5
5
5
5
5
5
5
5
5
5
5
5
5
5
5
5
5
5
5
5
5
5
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
iiilii!
< 0,400
< 0.400
< 0.600
< 0,600
< 0.208
< 0.208
< 1.52
< 1.52
< 0.960
< 0,960
< 0,400
< 0.400
< 1,20
« 1.20
< 0.400
< 0.400
< 1.60
< 1.60
< 0.920
< 0.920
< 0.280
< 0.280
iiisisws
< 0,400
< 0.600
< 0.208
< 1.52
< 0.960
< 0.400
< 1.20
< 0.400
< 1.60
< 0.920
< 0.280
HP
-
—
-
..
_
\ -•
:
„
«
/ I
-
:':->:-: *»fefitPjffi''"'-
•:-:-; -I'l^SsfH £*•>-:•• ,
-
—
_
_
_
-
-
-
„
-
-
-------
Client:
Proiect N
Pacifk Environmental Services
39568
Sample Report
Page 5 of 6
Date Received:
Date Prepared:
!?&?? Af^Y7-^t«
DATA FILE:
Matrix:
November 12-14, 1996
November 18-25, 1996
Nov^mlx^ 21-26. 1996
AR642. AB643 A AR644
Air
ANALYTE: Ha
ua/L RDU 0,2
Analysis Method:
29
Instrument- P F Zegmpn 51 OO
Spike Cone, lug^t
§
CVM ANALYTE SUMMARY REPORT
M29-1-ABHMS P'< D^a^, ••••
M29-1-ABHMSD <• kft
M29-1-BBHMS
M29-1-BBHMSD
M29-2-A BH MS
M29-2-A BH MSD
M29-2-B BH MS
M29-2-B BH MSD
M29-3-A BH MS
M29-3-A BH MSD
M29-3-B BH MS
M29-3-8 BH MSD
M29-5 BH MS
M29-5 BH MSD
M29-6 BH MS
M29-6BHMSD
M29-7 BH MS
M29-7 BH MSD
M29-1-A BH
M29-1-ABH
M29-1-BBH
M29-1-BBH
M29-2-A BH
M29-2-A BH
M29-2-B BH
M29-2-B BH
M29-3-ABH
M29-3-ABH
M29-3-8BH
14&4-1C MS
146-4-1C MSD
146-4-2DMS
146-4-2D MSD
146-4-3DE MS
146-4-3DE MSD
14&4-4DMS
146-4-4D MSD
146-4-5D MS
146-4-5D MSD
146-4-6DMS
146-4-6D MSD
146-4-8DEMS
146-4-8DE MSD
1464-9DE MS
1464-9DE MSD
146-4-10DE MS
1464-10DE MSD
True Spike MS
True Spike MSD
True Spike MS
True Spike MSD
True Spike MS
True Spike MSD
True Spike MS
True Spike MSD
True Spike MS
True Spike MSD
True Spike MS
True Spice MSD
IB)
5.436
5.291
5,507
5,621
5.926
5.459
5,604
5.818
4.896
4.893
4.871
4.860
4J97
4.617
2.751
3.424
4.175
4,178
5
5
5
5
5
5
5
S
5
5
S
5
m
900
900
970
970
960
960
680
680
900
900
860
860
1900
1900
1630
1630
1800
1800
900
900
970
970
960
960
680
680
900
900
860
860
fPPi
N/A
N/A
N/A
N/A
N/A
N/A
N/A
N/A
N/A
N/A
N/A
N/A
N/A
N/A
N/A
N/A
N/A
N/A
N/A
N/A
N/A
N/A
N/A
N/A
N/A
N/A
N/A
N/A
N/A
N/A
5
5
5
5
5
5
5
5
5
5
.5
5
5
5
5
5
5
5
5
5
5
5
5
5
5
5
5
5
5
5
IB
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
i
1
i
1
1
1
1
1
1
1
1
1
i
1
97.8
95.2
107
109
114
105
76.2
79.1
88.1
88.1
83.8
83,6
175
175
89.7
112
150.3
150.4
90.0
90.0
97.0
97.0
96.0
96,0
68.0
68.0
90.0
90.0
86.0
86,0
„
96.5
_
108
_
109
„_
77.7
—
88.1
„
83,7
*•
175
_
101
_
150.4
90.0
97.0
96.0
68,0
90,0
86.0
lili
2.70%
..
2.05%
™
8,20%
_
3.75%
~
0,061%
.-
0.226%
_
0,434%
_
21.8%
_
0.001
_
_
_
_
_
-
iflilj
104%
101%
105%
107%
114%
109%
107%
111%
98%
98%
97%
97%
92%
92%
/55%N
i, 68%,'
84%
84%
-
--
..
33
-------
Client
Project Number!
Pacific Environmental Services
39568
Sample Report
Pages of 6
Date Received:
Date Prepared:
IMte Ana^V7efk
DATA FILE:
^atpa,:
November 12-14, 1996
November 18-25, 1996
November 21-26. 1996
AB642. AB643 & AB644
Ak
ANALYTE: Ha
uafl. RDL 0.2
Anatvsis Msthod'
Instrument P E Zeqm
Spike Cone. tua/L\
29
an 5100
5
CVM ANALYTE SUMMARY REPORT
M29-58H
M29-58H
M29-6BH
M29-6BH
M29-7BH
M29-7BH
rf
Method Blank x«^< £p'"i//
Method Blank D v *s ' /
LCS \
LCSD \
Method Blank
Method Blank D
LCS
LCSD
Method Blank
Method Blank D
LCS
LCSD
Method Blank
Method Blank D
LCS
LCSD
Method Blank
Method Blank D
LCS
LCSD
True Spike MS
True Spike MSD
True Spike MS
True Spike MSD
True Spike MS
True Spike MSD
39568 MB1
39568 MB1D
39568 LCS1
39568 LCS1 D
39568 MB2
39568 MB2D
39568 LCS2
39568 LCS2D
39568 MBS
39568 MBS D
39568 LCS3
39568 LCS3D
39568 MB4
39568 MB4D
39568 LCS4
39568 LCS4D
39568AMB
39568AMBD
39568 A LCS
39568ALCSD
•H
5
5
5
5
5
5
0.026
0.033
5.078
5,137
0.003
0.003
4.706
4.885
-0.006
•0.008
4.372
4,515
0.025
0,020
4,762
4.751
-0.026
-0,026
4.876
5,152
liiii
1900
1900
1630
1630
1800
1800
_
-
_
-
_
-
—
-
—
-
_
»
_
-
„.
-
_
-
_
—
OTBI1
ippi
N/A
WA
N/A
N/A
N/A
N/A
„
~
„
_
_
_
„
-
—
-
-
' ™
_
_
_
_
_
—
••
5
5
5
5
5
5
_
-
„ ,
-
_
-
_
-
*~
-
_
-
__
-
—
-
_
-
—
—
sill
,.
1
1
1
1
1
_
-
_
-
_
-
_
_
—
-
_
_
—
_
_
_
_
_
**
—
190
190
163
163
180
180
_
-
_
-
_
-
_
-
-
„
-
_
-
_
-
_
-
—
—
.
190
^
163
„
180
„
-
_
-
-" -.
_
-
_
-
„
-
_
-
— ,
-
-
_
—
111!!
_
-
„
-
~
-
_
-
_
_
-'
_
_
_
-
_
_
-
».
_
_
_
-
--
„
I027r,
103%
--
94%
98%
--
87%
90%
--
95%
95%
--
98%
103%
Triangle Laboratories, Inc.
801 Captola Drive * Durham, North Carolina 27713
Tete: (919) 544-5729 * Fax; (919) 544-5491
Printed:
07-Dec-96 at 03:44 PM
-------
Central Park West
5001 South Miami Boulevard, P.O. Box 12077
Research Triangle Park, North Carolina 27709-2077
(919)941-0333 FAX: (919) 941-0234
Chain of Custody Record
e»
G
(
Project Number: S401
Project Name
EPA Lime Kiln Testing
Samplers:
Abernathy, Hamilton, Maret, Ritchie
Date
10/16/96
10/16/96
10/16/96
10/16/96
10/16/96
10/16/96
10/16/96
10/16/96
10/16/96
10/16/96
10/16/96
10/16/96
10/16/96
10/16/96
10/17/96
10/17/96
10/17/96
Time
20:40
20:40
20:40
20:40
20:40
20:40
20:40
20:40
20:40
20:40
20:40
20:40
20:40
20:40
16:45
16:45
16:45
10/17/96 16:45
Field Sample 10
M29-1-A-AR2
M29-1-A-F1
M29-1-A-FH3
M29-1-A-BH4
M29-1-A-5A
M29-1-A-5B
M29-1-A-5C
M29-1-B-AR2
M29-1-B-F1
M29-1-B-FH3
M29-1-B-BH4
M29-1-B-5A
M29-1-B-5B
M29-1-B-5C
M29-2-A-AR2
M29-2-A-F1
M29-2-A-FH3
M29-2-A-BH4
ReiiKqtjtefc£<£by:
;/-/*-#
Sample Description
FH Acetone Rinse
Filters - 2
FH0.1NHNO3 rinse
Impingers 1 , 2, & 3 contents and rinses
Impinger 4 rinse
Impingers 5 & 6 rinses
Impingers 5 & 6 8N HCI rinse
FH Acetone Rinse
Filters - 3
FH0.1NHNO3 rinse
Impingers 1, 2, & 3 contents and rinses - 2
Impinger 4 rinse
Impingers 5 & 6 rinses
Impingers 5 & 6 8N HCI rinse
FH Acetone Rinse
Filters - 2
FH0.1NHNO3 rinse
Impingers 1, 2, & 3 contents and rinses
Analysis Requested
Metals
*
.«
*
*
•
*
*
•
*
*
*
*
•
*
Hg
•
•
•
•
•
•
*
•
•
•
•
•
•
*
•
*
•
•
Deceived by: (Signature) Relinquished by: (Signature)
^^^4^^
-------
ENVIRONMENTAL SERVICES. INC.
Central Park West
5001 South Miami Boulevard, P.O. Box 12077
Research Triangle Park, North Carolina 27709-2077
(919) 941-0333 FAX: (919) 941-0234
Chain of Custody Record
£
»-
(
Project Number: S401
Project Name
EPA Lime Kiln Testing
Samplers:
Abernathy, Hamilton, Maret, Ritchie
Date
10/17/96
10/17/96
10/17/96
10/17/96
10/17/96
10/17/96
10/17/96
10/17/96
10/17/96
10/17/96
10/18/96
10/18/96
10/18/96
10/18/96
. 10/18/96
10/18/96
10/18/96
10/18/96
Time
16:45
16:45
16:45
16:45
16:45
16:45
16:45
16:45
16:45
16:45
16:00
16:00
16:00
16:00
16:00
16:00
16:00
16:00
Field Sample ID
M29-2-A-5A
M29-2-A-5B
M29-2-A-5C
M29-2-B-AR2
M29-2-B-F1
M29-2-B-FH3
M29-2-B-BH4
M29-2-B-5A
M29-2-B-5B
M29-2-B-5C
M29-3-A-AR2
M29-3-A-F1
M29-3-A-FH3
M29-3-A-BH4
M29-3-A-5A
M29-3-A-5B
M29-3-A-5C
M29-3-B-AR2
Ratmfluished by: (Signature)
Relinquished by: (Signature)
k
^ ii Hfc.
RelTno^BrfftdWuSigfiaturS
•-Jj&M/
^^J\_S\s\J/
Date/Time
f«prn?
\3-u> (.
Date/Time
Date/Time
/£.'V*»
\Hl^L
Sample Description
Impinger 4 rinse
Impingers 5 & 6 rinses
Impingers 5 & 6 8N HCi rinse
FH Acetone Rinse
Filter
FH0.1NHNO3 rinse
Impingers 1, 2, & 3 contents and rinses
Impinger 4 rinse
Impingers 5 & 6 rinses
Impingers 5 & 6 8N HCI rinse
FH Acetone Rinse
Filters - 2
FH0.1NHNO3 rinse
Impingers 1 , 2, & 3 contents and rinses
Impinger 4 rinse
Impingers 5 & 6 rinses
Impingers 5 & 6 8N HCI rinse
FH Acetone Rinse
Received by: (Signature)
^^yr7 /
~-r* S'f~C***^+ —
Received by: (Signature)
Received for lab by: (Signature)
c.
-------
RONMENTAL SERVICES. INC.
Central Park West
5001 South Miami Boulevard, P.O. Box 12077
Research Triangle Park, North Carolina 27709-2077
(919)941-0333 FAX: (919) 941-0234
Chain of Custody Record
£
(
(
Project Number S401
Project Name
EPA Lime Kiln Testing
Samplers:
Abemathy, Hamilton, Maret, Ritchie
Date
10/18/96
10/18/96
10/18/96
10/18/96
10/18/96
10/18/96
10/19/96
10/19/96
10/19/96
10/19/96
10/19/96
10/19/96
10/19/96
10/19/96
10/19/96
10/19/96
10/19/96
10/19/96
Time
16:00
16:00
16:00
16:00
16:00
16:00
13:30
13:30
13:30
13:30
13:30
13:30
13:30
16:00
16:00
16:00
16:00
16:00
Field Sample ID
M29-3-B-F1
M29-3-B-FH3
M29-3-B-BH4
M29-3-B-5A
M29-3-B-5B
M29-3-B-5C
M29-4-AR2
M29-4-F1
M29-4-FH3
M29-4-BH4
M29-4-5A
M29-4-5B
M29-4-5C
M29-5-AR2
M29-5-F1
M29-5-FH3
M29-5-BH4
M29-5-5A
toHogujstacI by: (Signature)
Relinquished by: (Signature)
2
** .• ^
RelinqUhtKi-^:£$iga^ture)
DateflMe
IQM%
(t'O"
Date/Time
Pate/Time
/Z.'VD
I/-K-9L
Sample Description
Filter
FH0.1NHNO3 rinse
Impingers 1 , 2, & 3 contents and rinses - 2
Impinger 4 rinse
Impingers 5 & 6 rinses
Impingers 5 & 6 8N HCI rinse
FH Acetone Rinse
Filters - 2
FH 0.1N HNO3 rinse
Impingers 1 , 2, & 3 contents and rinses - 3
Impinger 4 rinse
Impingers 5 & 6 rinses
Impingers 5 & 6 8N HCI rinse
FH Acetone Rinse
Filters - 2
FH0.1NHNO3 rinse
Impingers 1 , 2, & 3 contents and rinses - 2
Impinger 4 rinse
Received by: (Signature)
^^^^^^
Deceived by: (Signature)
Received for lab by: (Signature)
<^t£j}p*.
Analysis Requested
Metals
*
'•
•
*
*
«
•
•
*
•
*
•
•
*
Hg
•
*
•
•
*
•
•
*
*
•
*
•
•
*
*
*
*
•
Relinquished by: (Signature)
'^^^^^_
Relinquished by: (Signature
Date/Time
^/Z
-------
RONHEKTAL SERVICES. INC.
Central Park West
5001 South Miami Boulevard, P.O. Box 12077
Research Triangle Park, North Carolina 27709-2077
(919) 941-0333 FAX: (919) 9414)234
Chain of Custody Record
i
ft
I
Project Number: S401
Project Name
EPA Lime Kiln Testing
Samplers:
Abernathy, Hamilton, Maret, Ritchie
Date
10/19/96
10/19/96
10/20/96
10/20/96
10/20/96
10/20/96
10/20/96
10/20/96
10/20/96
10/20/96
10/20/96
10/20/96
10/20/96
10/20/96
10/20/96
10/20/96
10/20/96
. 10/20/96
Time
16:00
16:00
12:30
12:30
12:30
12:30
12:30
12:30
12:30
15:00
15:00
15:00
15:00
15:00
15:00
15:00
15:00
15:00
Field Sample ID
M29-5-5B
M29-5-5C
M29-6-AR2
M29-6-F1
M29-6-FH3
M29-6-BH4
M29-6-5A
M29-6-5B
M29-6-5C
M29-7-AR2
M29-7-F1
M29-7-FH3
M29-7-BH4
M29-7-5A
M29-7-5B
M29-7-5C
M29-FB-AR2
M29-FB-F1
teliflfluished by: (Signatfire)
^^
Relinquished by: (Signature)
^MHMrtiiif'HatfM — '*" •*
"pfWHBiiwrr
"-TVX^
flr- «W"W<»J
t^r, /^
uO iw
Date/Tirte
ifo ft
(?W '
Date/Time
Date/Time
& .'y»
(-/L-9L.
Sample Description
Impingers 5 & 6 rinses
Impingers 5 & 6 8N HCI rinse
FH Acetone Rinse
Filters - 2
FH0.1NHNO3 rinse
Impingers 1, 2, & 3 contents and rinses - 2
Impinger 4 rinse
Impingers 5 & 6 rinses
Impingers 5 & 6 8N HCI rinse
FH Acetone Rinse
Filters - 2
FH0.1NHNO3 rinse
Impingers 1, 2, & 3 contents and rinses - 2
Impinger 4 rinse
Impingers 5 & 6 rinses
Impingers 5 & 6 8N HCI rinse
FH Acetone Rinse
Filters - 2
Analysis Requested
Metals
*
*
•
*
*
•
*
*
•
*
•
•
Hg
*
•
*
*
•
•
*
*
*
•
*
*
•
•
*
*
*
•
1
Received by: (Signature) Relinquished by: (Signature)
/^^^_ '<^^~^-^
Received by: (Signature) Relinquished by: (Signature)
DatefTime/
'0/*A&
0300
Date/Time
Received for lab by: (Signature) REMARKS
~ . A Metals Target List: Sb, As, Be, Cd, Cr, Co, Pb, Mn, 1
jf 4gf A.J It
c. f, tf yL-*-o2<*-)
Remarks
Beaker No. 117
Beaker No. 118
Beaker No. 119
Beaker No. 120
FIELD BLANK - Beaker No. 121
FIELD BLANK - Beaker No. 122
Ree%fijtw: (Sipnatrfre)
^&UW
Received by: (Signature)
%Se
|Pafle:__4__ of 9
-------
>ACinC ENVIRONMENTAL SERVICES. INC.
Central Park West
5001 South Miami Boulevard, P.O. Box 12077
Research Triangle Park, North Carolina 27709-2077
(919) 941-0333 FAX: (919) 941-0234
Chain of Custody Record
Project Number: S401
Project Name
EPA Lime Kiln Testing
Samplers:
Abernathy, Hamilton, Maret, Ritchie
Date
10/20/96
10/20/96
10/20/96
10/20/96
10/20/96
10/20/96
10/20/96
10/20/96
10/20/96
10/20/96
10/20/96
10/20/96
10/21/96
10/21/96
10/21/96
10/21/96
10/21/96
10/21/96
Time
15:00
15:00
15:00
15:00
15:00
15:00
15:00
15:00
15:00
15:00
15:00
15:00
14:00
14:00
14:00
14:00
14:00
14^00
Field Sample ID
M29-FB-FH3
M29-FB-BH4
M29-FB-5A
M29-FB-5B
M29-FB-5C
M29-RB-AR2
M29-RB-F1
M29-RB-FH3
M29-RB-BH4
M29-RB-5A
M29-RB-5B
M29-RB-5C
M29-10-AR2
M29-10-F1
M29-10-FH3
M29-10-BH4
M29-10-5A
M29-10-5B
RSsqaiBsfftMl by: jStgntfture)
^SSZJr
Relinquished by: (Signature)
ReTlnIfi6iBj|y^ignjJure)
^MuJ^
Data/Tin/*,
lt>f?f(V
P*> ^
Analysis Requested
Metals
*
•
*
*
*
*
*
•
•
*
*
•
*
Hg
*
•
*
*
•
•
*
•
•
•
•
*
•
*
*
•
•
•
-
Relinquished by: (Signature)
'^7?£~^-
Relinquished by: (Signature)
DatefTim/
/e*/&7$k.
O9PV
Date/Time
Remarks
FIELD BLANK
FIELD BLANK
FIELD BLANK
FIELD BLANK
FIELD BLANK
REAGENT BLANK -Beaker 123
REAGENT BLANK - Beaker 124
REAGENT BLANK
REAGENT BLANK
REAGENT BLANK
REAGENT BLANK
REAGENT BLANK
Beaker No. 125
Beaker No, 126
if
Rt^Stby: JSignafure)
-Whs
Received by: (Signature)
REMARKS
Metals Target List: Sb, As, Be, Cd, Cr, Co, Pb, Mn, Ni, Se
|Page:_5_ of 9
-------
RONMENTAL SERVICES. INC.
Central Park West
5001 South Miami Boulevard, P.O. Box 12077
Research Triangle Park, North Carolina 27709-2077
(919) 941-0333 FAX: (919) 941-0234
Chain of Custody Record
I
c
(
Project Number: S401
Project Name
EPA Lime Kiln Testing
Samplers:
Abernathy, Hamilton, Maret, Ritchie
Date
10/21/96
10/21/96
10/21/96
10/21/96
10/21/96
10/21/96
10/21/96
10/21/96
10/21/96
10/21/96
10/21/96
10/21/96
10/21/96
10/21/96
10/21/96
10/22/96
10/22/96
10/22/96
Time
14:00
16:30
16:30
16:30
16:30
16:30
16:30
16:30
17:00
17:00
17:00
17:00
17:00
17:00
17:00
18:00
18:00
18:00
Field Sample ID
M29-10-5C
M29-11-AR2
M29-11-F1
M29-11-FH3
M29-11-BH4
M29-11-5A
M29-11-5B
M29-11-5C
M29-12-AR2
M29-12-F1
M29-12-FH3
M29-12-BH4
M29-12-5A
M29-12-5B
M29-12-5C
M29-13-I-AR2
M29-13-I-F1
M29-13-I-FH3
fteJttauUttd by: (SignaJUre)
Relinquished by: (Signature)
fieUfwaii^by: (SiWure
^gl^
Data/Time
iJtxw
Mo <
DatefTime
Date/Time
yi.'V*-
U-&-9L
Sample Description
Impingers 5 & 6 8N HCI rinse
FH Acetone Rinse
Filters - 2
FH 0.1 N HNO3 rinse
Impingers 1, 2, & 3 contents and rinses
Impinger 4 rinse
Impingers 5 & 6 rinses
Impingers 5 & 6 8N HCI rinse
FH Acetone Rinse
Filters - 2
FH 0.1 N HNO3 rinse
impingers 1, 2, & 3 contents and rinses
Impinger 4 rinse
Impingers 5 & 6 rinses
Impingers 5 & 6 8N HCI rinse
FH Acetone Rinse - 2
Filters - 2
FH 0.1 N HNO3 rinse
Received by: (Signature)
-'"^^^/7 /
_-~#^ /X/*^*^'*^
Received by: (Signature)
Received for lab by: (Signature)
c<£ &it*
Analysis Requested
Metals
, •
•
•
*
•
*
*
•
•
*
•
•
»
Hg
*
*
*
•
*
•
*
*
*
•
' *
•
*
*
•
•
*
*
Relinquished by: (Signature)
^(^^%^<£^
Relinquished by: (Signature)
Dateffimef
4)/ttf$
f^6p
Date/Time
Remarks
Beaker No. 127
Beaker No. 128
Beaker No. 129
Beaker No. 130
Beaker No. 131 - NOT INCLUDE
Beaker No/tf2j>
Reg&hrtSW (Signatujfe)
l/(-S \s\ff
Received by: (Signature)
REMARKS
Metals Target List: Sb, As, Be, Cd, Cr, Co, Pb, Mn, Ni, Se
iPage: 6 of 9
-------
PACIFIC ENVIRONMENTAL SERVICES. INC.
Central Park West
5001 South Miami Boulevard, P.O. Box 12077
Research Triangle Park, North Carolina 27709-2077
(919) 941-0333 FAX: (919) 941-0234
Chain of Custody Record
i
c
(
Project Number: 8401
Project Name
EPA Lime Kiln Testing
Samplers:
Abernathy, Hamilton, Maret, Ritchie
Date
10/22/96
10/22/96
10/22/96
10/22/96
10/22/96
10/22/96
10/22/96
10/22/96
10/22/96
10/22/96
10/22/96
10/23/96
10/23/96
10/23/96
10/23/96
10/23/96
10/23/96
10/23/96
Time
18:00
18:00
18:00
18:00
18:00
18:00
18:00
18:00
18:00
18:00
18:00
16:00
16:00
16:00
16:00
16:00
16:00
16:00
Field Sample ID
M29-13-I-BH4&5A
M29-13-l-BH4-Filtrate
M29-13-I-5B
M29-13-I-5C
M29-13-O-AR2
M29-13-O-F1
M29-13-O-FH3
M29-13-O-BH4
M29-13-O-5A
M29-13-O-5B
M29-13-O-5C
M29-14-I-AR2
M29-14-I-F1
M29-14-I-FH3
M29-14-I-BH4
M29-14-I-5A
M29-14-I-5B
M29-14-I-5C
R3toiqiu*had by: (Signature)
^yStJ'
Relinquished by: (Signature)
Mb. »—-
q^^
Date/Time
tohm
(?£& *
Date/Time
Date/Time
)t;
-------
ENVIRONMENTAL SERVICES. INC.
Central Park West
5001 South Miami Boulevard, P.O. Box 12077
Research Triangle Park, North Carolina 27709-2077
(919) 941-0333 FAX: (919) 941-0234
Chain of Custody Record
Project Number: S401
Project Name
EPA Lime Kiln Testing
Samplers:
Abemathy, Hamilton, Maret, Ritchie
Date
10/23/96
10/23/96
10/23/96
10/23/96
10/23/96
10/23/96
10/23/96
10/24/96
10/24/96
10/24/96
10/24/96
10/24/96
10/24/96
10/24/96
10/24/96
10/24/96
10/24/96
10/24/96
Time
16:00
16:00
16:00
16:00
16:00
16:00
16:00
17:30
17:30
17:30
17:30
17:30
17:30
17:30
17:30
17:30
17:30
1PJ.-30
Field Sample ID
M29-14-O-AR2
M29-14-O-F1
M29-14-O-FH3
M29-14-O-BH4
M29-14-O-5A
M29-14-O-5B
M29-14-O-5C
M29-15--AR2
M29-15--F1
M29-15--FH3
M29-15--BH4
M29-15--5A
M29-15--5B
M29-15--5C
M29-15-O-AR2
M29-15-O-F1
M29-15-O-FH3
M29-15-O-BH4
Relinquished by (SidVature)
Relinquished by: (Signature)
!!^7^
Date/Time
/o/2Spf
/?#> <•
Date/Time
Date/Time
JL;V*
il~tL"
-------
AL SERVICES. INC.
Central Park West
5001 South Miami Boulevard, P.O. Box 12077
Research Triangle Park, North Carolina 27709-2077
(919)941-0333 FAX: (919) 941-0234
Chain of Custody Record
(
,f
c
Project Number: S401
Project Name
EPA Lime Kiln Testing
Samplers:
Abernathy, Hamilton, Maret, Ritchie
Date
10/24/96
10/24/96
10/24/96
10/25/96
10/25/96
10125m
10/25/96
10/25/96
10/25/96
10/25/96
10/25/96
10/25/96
10/25/96
10/25/96
10/25/96
10/25/96
10/25/96
Time
17:30
17:30
17:30
10:00
10:00
10:00
10:00
10:00
10:00
10:00
10:00
10:00
10:00
10:00
10:00
10:00
10:00
Field Sample ID
M29-15-O-5A
M29-15-O-5B
M29-15-O-5C
M29-16-AR2
M29-16-F1
M29-16-FH3
M29-16-I-BH4
M29-16-5A
M29-16-5B
M29-16-5C
M29-17-AR2
M29-17-F1
M29-17-FH3
M29-17-BH4
M29-17-5A
M29-17-5B
M29-17-5C
BaMBMiedby; (Signature)
Relinquished by: (Signature)
Ke?[r)c}uis>p3Tw: (Sjlpalufi)
{of?$/w
I7ff(> <
Date/Time
Date/Time
)i [tf*
)I~/L-$L
Sample Description
Impinger 4 rinse
Impingers 5 & 6 rinses
Impingers 5 & 6 8N HCI rinse
FH Acetone Rinse
Filters
FH 0.1 N HNO3 rinse
Impingers 1, 2, & 3 contents and rinses
Impinger 4 rinse
Impingers 5 & 6 rinses
Impingers 5 & 6 8N HCI rinse
FH Acetone Rinse
Filters - 2
FH 0.1 N HNO3 rinse
Impingers 1,2, & 3 contents and rinses
Impinger 4 rinse
Impingers 5 & 6 rinses
Impingers 5 & 6 8N HCI rinse
Deceived by: (Signature)
X"^J
-------
c
USB ',
/g/ PACIFIC ENVIRONMENT
Project Number S«1
,
U_ SERVICES. INC.
Central Park West
5001 South Miami Boulevard, P.O. Box 12077
Research Triangle Park, North Carolina 27709-2077
(9 1 9) 94 1 -0333 FAX: (9 1 9) 94 1 -0234
Chain of Custody Record
Project Name
EPA Lime Kiln Testing
Samplers:
Abernathy, Hamilton, Marat, Ritchie
Date
10/16V96
10/22/96
10/23/96
KU24/99
Time
20:40
18:00
16:00
— "T7T38
»
Field Sample ID
M29-1-A-F1
M29-13-I-AR2
M29-14-I-AR2
M29-4S-Wtf*2--
-J/^iW
^•linqulihed by: (Signature)
5
^*~*^s"\/vl If
Date/Tidie
Date/Tuna
Dafe/Tlme
Sample Description
Filters - 2
FH Acetone Rinse - 2
FH Acetone Rinse
gH-A6etane-Btasa —__—-• — -—
Received by: (Signature)
Received by^(Signatufei , —
Received for lab by: (Sigfiatdre)
rjKj^ty/ yy?^*?
Analysis Requested
Metals
*
*
•
— «—
Hg
•
*
*
*
_— —
— ~_
Relinquished by: (Signature)
Relinquished by: (Signaluie)
_-—-
— —^
Datertim^'
$\u)
Date/Time
Remarks
Beaker No. 102
Beaker No. 131
Beaker No. 136
Beaker-Ner44Q
.
k
«-,
flgo^ed bY (aignaAre)
Received by: (Signature)
REMARKS
Metals Target List. Sb. As, Be, Cd, Cr, Co, Pb, Mn, Ni, Se
(Page: i_.of 1
-------
PACIFIC ENVIRONMENTAL SERVICES. INC.
Central Park West
5001 South Miami Boulevard, P.O. Box 12077
Research Triangle Park, North Carolina 27709-2077
(919) 941-0333 FAX: (919) 941-0234
Chain of Custody Record
n
/
•• —
Project Number: S401
Project Name
EPA Lime Kiln Testing
Samplers:
Abernathy, Hamilton, Maret, Ritch e
Date
i
10/24/96
1
This
. '••• .1
17:30
Field Sample ID
M29-1&-I-AR2
Relinquished by: (Signature)
Relinquished by: (Signature)
RetffiqU«Tied by: (Signature)
^XJv'^
DateATime
Date/Time
Date/Tirna
Y* h
her
Sample Description
FH Acetone Rinse
Received by: (Signature)
Received by: (Signature)
Received for lab by: (Signature) . lay
s f ~i t ' //M/ r^-
t 4 , -ii. • ; ' /' I1 J—
~f '•'"•" i?;^
Analysis Requested
Metals
•
Hg
*
Relinquished by: (Signature)
Relinquished by: (Signature)
Date/Time
Date/Time
Remarks
Beaker No. 140
Received by: (Signature)
Received by: (Signature)
REMARKS
Metals Target List: Sb, As, Be, Cd, Cr, Co, Pb, Mn, Ni, Se
iPage: i or 1
-------
PASE 1 OF
: Custody Seal : Absent
Chain of Custody : Present
: Saiole Tags ; Present
! Sanole Tag Numbers: Listec
; SMO Fons ; N/A
1 3ox
: TLI Nuaber flatrix
I iR/H:CPM Client ID Location
1 146-4-1A FH ACETONE RNC
! fl29-i-A-«R2
: METALS LAB
I 146-4-18 , FH.IHHHO:
! ,129-1-A-FH3
: MCTALS LAB
! 146-4-1C IMP 1.2.3
! M29-1-A-8H4
METALS LAB
1 146-4-10 IMP4
: ,129-l-A-SA
I METALS LAE
I 146-4-1E IMP 5,fc
: (129-1-A-5B •
I METALS LAE
1 146-4-lF IMP 5.6 HC1
! ,129-1-A-SC
1 METALS LAB
I 146-4-2A FILTER
! M29-1-8-F1
1 . METALS LAE
I 146-4-2B FH ACETONE RKS
! H29-1-8-AR2
! METALS LAB
! 146-4-2C FH .1H HK03
! M29-1-8-FH3
! BETALS LAB
! 146-4-20 IMP 1.2.3
! M29-1-8-8H4
METALS LAB
: Receiving ReiarKs:
t
i
Saiole Seals; Absent : TLI
...*..**.*-MI..£^i
Proisci Hui0er I
: Client: PES03 !
' Date
Received :
rtO COOLANT 1 Carrier and Nunber !
: TO LAB : TO STORAGE: TO LAB :
1 Date/Init I Oate/Init ! Date/Init !
f I i !
1 i I i
!._-.._-. --,.4,-. -----.. ,-.i-.»«»,--.-»-4..
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1 1 1 1
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.A-. — ...... ..{.. **....«...»}*-. — ,..--. — f
1 1 i I
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39563
.. ...s......
; Book ;
Pacific Enyironiental Services : 146 1
11/12/96
J£HE RILEY
To STORAGE! To LAB 1 To
Oate/Init ! Cate/Init ! Oa
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STORAGE! Ta ARCHIVE:
te/Init i Oate/Init !
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;
1 :
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DISPOSED :
Date/Init ,'
;
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Archive ReiarKs:
-TRIANGLE LABORATORIES. INC.-LOG IN RECORD/CHAIN OF CUSTODY-REVISED 06/11/1996-
51
-------
: Custody Seal : Absent
! Chain of Custody : Present
! Saiole Tags : Present
! Saiole Tag Numbers: Listec
! SMO ForiBS : N/A
! 3ox
: TLI Nuflbar Matrix
! ifi/H:CPM Client ID Location
! 146-4-2E IHP 4
i H29-1-B-SA
! METALS LAB
! 146-4-2F ' IMP 5.6
! I129-1-B-5B
! METALS LAB
! 146-4-2S IMP 5.6 HCi
; 129-1-8-5C
! ' METALS LAB
! 146-4-3A - FILTER
, Fu7 fc"H*F 1
METALS LAB
! 146-4-3B FK ACETONE RNS
! f129-2-fi-AS2
! METALS LAO
! 146-4-3C FH .IK HN03
! N29-2-A-FH3
i MEMS LAB
! 146-4-3D IMP 1.2.3
! M29-2-A-8H4
! METALS LAB
! 146-4-3E IMP 1.2.3
i H29-2-A-8H4
! HETALS LAB
! 146-4-3F IMP 4
! M29-2-A-5A
1 . METALS LAB
! 146-4-36 IHP S.t
! M29-2-A-58
I METALS LAB
! Receiving Raiarks:
i
Saiole
Accent
NO COOLANT
t — 1-
! To LfiB !
! Date/Init !
1 1
! 1
1 1
i i
f 1
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i $
• i
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.Cond.; YES
int ! TLI Project Nmbir !
: Client: PESOS
1 Date Received
i
! Carrier and Nuiber I
To STORAGE!
Date/Init !
i
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1
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Dats/Init ! Oate/Init
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1
i
PAGE 2 OF 17
39568
Pacific
11/12/96
Environmental Services
!8y^M^/i
JENE RILEY
T..*** T.
! To LA8 I
! Date/Init !
1
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Date/Init ! Date/Init
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1
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1
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! 146
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; 4
! DISPOSED
! Date/ Ink
1
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-TRIANGLE LABORATORIES. IHC.-LOG IN RECORD/CHAIN OF CUSTODY-REVISED 06/13/1996 J-~ t
-------
PAGE 3 OF 17
t
Custody Seal : Absent
Chain of Custody : Present
Saiole Tags : Present
Saiole Tag Numbers: Listed
SMO Foris : N/A
Box
Saaole Seals: Absent
Accent. Cond.: YES
•T- — - — "- — --f .-._ --....-.,-|.
! TLI Project Huiber ! 39S68 ;
! Client: PES03 ! Pacific Envjconiental Services !
! Date Received ! 11/12/96 ! By A/)/L A /\/\/'<
„_,_ . j. .. . j. j._ 1/1 /fn/i/f *
NO COOLANT
TLI Nuaber Matrix
«R/H:CPM Client ID Location
146-4-3H IMP 5.6
M29-2-A-5C
METALS
HC1
LAB
146-4-4A ' FILTER
METALS
146-4-4E FH ACETONE
n27-2"B-MK2
METALS
146-4-4C FH .IN h
M29-2-B-FH3
METALS
146-4-4D IMP 1
(129-2-B-BH4
METALS
LAB
RNS
LAE
N03
LAD
1 7
L, t O
LAE
146-4-4E IMP 4
M29-2-8-5A
METALS
146-4-4F IMP
M29-2-8-SB
METALS
146-4-4G IMP 5.6
METALS
LAB
S.6
LAB
HC1
LAB
146-4-5A FILTER
METALS
146-4-5B FH ACETONE
M29-3-A-AR2
METALS
Receiving Reiarks:
Archive Reaarks:
LAB
RNS
LAB
: Carrier and Nuiber ! JENE RILEY
7"V" »
1
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Book [
L46 !
Page ;
4 J
! TO LAS : TO STORAGE: TO LAB : TO STORAGE: TO LAB : TO STORAGE: TO ARCHIVE; DISPOSED :
! Date/Init ! Date/Init ! Date/Init ! Oate/Init ! Date/Init ! Date/Init ! Oate/Init 1 Oate/Init \
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-TRIANGLE LABORATORIES. INC.-LOG IN RECORD/CHAIN OF CUSTODY-REVISED 06/13/1996
-------
PAGE 4 OF 17
Custody Seal : Absent San
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Chain of Custody : -Present Accent
Saiole Tags : Present
Saiols Taa Nunbers: -listsd
SMO Foras : N/A
Box NO COOLANT
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54
-------
PAGE S OF 17
*
Custody
Chain of
Seal :
Custody :
SaiDle Taas :
SMO foris :
Sox _
TLI Number
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146-4-6F
146-4-6B
146-4-7A
146-4-7E
146-4-7C
146-4-70
146-4-7E
146-4-7F
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-TRIANGLE LABORATORIES. IHC.--LQS IN RECORD/CHAIN OF CUSTODY-REVISED 06/13/1996 '
-------
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Saide Tags :
Saaole Tag Huioers:
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146-4-8A
146-4-8B
146-4-8C
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146-4-8E
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146-4-8G
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M29-5-BH4
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H29-5-5A
H29-5-58
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Enuironiental Services
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-TRIANGLE LABORATORIES. INC.-LOG IN RECORD/CHAIN OF CUSTODY-REVISED 06/13/1996
-------
PAGE 7 OF 1?
Custody Seal : Absent Saiuli Seals: Absi
Chain of Custody : Present Acceot.Cond,: YES
Saaole Tags : Present
Sasflle Taa Nui&ers: Listed
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146-4-9E IMP 1,2.3 !
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146-4-9F IMP 4 !
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146-4-9H IMP 5.6 KC1 !
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146-4-1QA FILTER !
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146-4-10B FH ACETOME RHS !
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57
-------
PAGE 8 OF 17
(.
Custody Seal : Absent
Chain of Custody : Present
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146-4-11A FILTER !
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146-4-11C FH .IN HH03 !
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146-4-11D IMP 1,2.3 !
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146-4-11E IMP 4 !
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Archive Reiarks:
-TRIANGLE LABORATORIES. IHC.-LOG IN RECORO/CHAIK OF CUSTOOY--REVISEO 06/13/1996-
53
-------
Custody Seal :
Chain of Custody :
Saiole Tags :
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Box
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Absent .
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-TRIANGLE LABORATORIES. IHC.--L06 IH RECORD/CHAIN OF CUSTODY--REVISED 06/13/1996-
-------
PAGE, i or
Custoov Seal : Present/Intact
Cniin of Custody : Present
£auis Tags : Present
Saule Tag Huioers: Lisiec
SflQ Forts : N/A
Saioie Seals: Present ! TLI Proiect Nuioer : 39190
Acceot.Conc.; YES -
i Client: PESC3 : Pacific Environiintal Services
+ »
! Date Received I 11/14/96 ! 8v >
: BOOK ;
; 146 !
: Pane !
Sox
00 COOLANT
! Carrier and Nuuer : ROBERT DAVIS
26
: TLI Huioer
! iR/H;CPI! Client ID
! 146-26-1
A «29-l-A-Fl:8EAKER
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Location
BEAKEP.
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METALS LAE
! .146-26-2 BEAKER
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-------
Projecl f
T"an9'e Laboratories of RTP.-INC.
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Triangle Laboratories of RTP, INC.
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Triangle Laboratories "of RTP.-INC.
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Projec!
Triangle Laboratories of RTP/INC.
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Triangle Laboralorles of RTPrINC,
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-------
PAGE
15
INORGANICS SPIKE LOG
DATE
PROJECT #
SAMPLERS
ANALVTE
ORIGINAL
STANDARD
#
ORIGINAL
STANDARD
CONG.
(PPM)
SPIKE
SAMPLE
RNAL
VOLUME
SPIKE
SAMPLE
(PPB)
INITIALS
WITNESS
looo,,
'loo
4
(000^
/CO
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74
-------
SEE SPIKE LOG
Spiking Standard Preparation
Element Standard Orig. Sid. SDika(uL) cone
10 (ppm)
*g
Ja
Ja
Mi
sb
Sb
>e
5
n
Zn
Zn
2-1 00-5
2-100-4
2-100-5
2-105-7
2-100-5
2-100-5
2-100-4
2-100-4
2-105-S
2-100-4
2-100-4
2-100-4
2-1 00-4
2-100-4
2-1 05-9
2-100-5
2-108-7
2-100-4
2-106-1
2-100-4
2-100-4
2-1 00-5
2-108-6
2-100-4
2-100-4
2-100-4
2-100-4
2-100-4
2-100-4
2-100-4
2-100-4
2-106-5
100
100
100
10000
100
100
100
100
10000
100
100
100
100
100
10000
1000
10000
100
10000
100
100
100
10000
100
100
100
100
100
100 .
100
100
1000
FvoldOOmL) (ppm)
5000
5000
5000
950
5000
5000
5000
5000
950
5000
5000
5000
5000
5000
950
5000
1500
5000
950
5000
5000
5000
1950
5000
5000
5000
5000
5000
5000
5000
5000
1500
5
5
5
95
5
5
5
5
95
5
5
5
5
5
95
50
150
5
95
5
5
5
195
5
5
5
5
5
5
5
5
15
SPIKING
'rom Spiking Standard
Spike(uL) cone
^olflOOmi) (ppb)
1000
1000
1000
1000
1000
1000
1000
1000
1000
1000
1000
1000
1000
1000
1000
1000
1000
1000
1000
1000
1000
1000
1000
1000
1000
1000
1000
1000
1000
1000
1000
1000
50
50
50
950
50
50
50
50
950
50
50
50
50
50
950
500
1500
50
950
50
50
50
1950
SO
50 »
50
50
50
50
50
50
150
combined
totsi
1000
1000
1000
2000
1000
2000
200
"Spike seperat*ty
Element Orig Std SpQcB(uL) cone
(ppm) Fvol(100 (ppb)
Au
C«
U
P
Pd
ft
S
Si
Sn
Sr
1000
1000
1000
1000
TOOT,
1000
1000
10000
1000
1000
140
30
70
100
160
~CO
350
350
20
5
1400
300
700
1000
1SOU
lOOO
35CJ
35000
200
50
10OOuL of the Spiking Standard gives tne listed cone, of the above elements.
Spiking Standard 2-1 10-3
Spiked by: A. A
Predtgestion- \^r^P
Postdigestiorv-
-------
INORGANICS SRKE LOG
PAGE \b
DATE
PROJECT #
SAMPLE IDs
ANALYTE
ORIGINAL
STANDARD*
ORIGINAL
STANDARD CONC.
(PPM)
SPIKE
SAMPLE
(Hi.)
FINAL
VOLUME
(mL)
SPIKE
SAMPLE
(PPB)
INITIALS
WITNESS
37-55-j*
W 757/1
6 eft
V
-its
Wfr1/
-us
f»A5f)
LIU
FORM # 0101-16 (06/12/96)
'
76
-------
* SEE SPIKE LOG
Spiking Standard Preparation
Element Standard Orig. Std. Spike(uL) cone
ID (ppm)
*g
4.S
41
4,1
3
3a
3a
;a
Sa
;d
So
2r
;u
:e
:6
<
>
\
*g
dg
dn
*10
•Ja
Ma
1i
5b
Sb
SO
1
n
(/
Zn
Zn
2-100-5
2-100-4
2-100-S
2-105-7
2-100-5
2-1 00-5
2-100-4
2-100-4
2-105-a
2-100-4
2-100-4
2-100-4
2-1 00-4
2-100-4
2-105-9
2-100-5
2-108-7
2-1 00-4
2-106-1
2-100-4
2-100-4
2-1 00-5
2-108-6
2-1 00-4
2-100-4
2-100-4
2-100-4
2-100-4
2-100-4
2-100-4
2-100-4
2-1 06-5
100
100
100
10000
100
100
100
100
10000
100
100
100
100
100
10000
1000
10000
100
10000
100
100
100
10000
100
100
100
100
100
100
100
100
1000
Fvolfl 00ml) (ppm)
5000
5000
5000
950
5000
5000
5000
5000
950
5000
5000
5000
5000
5000
950
5000
1500
5000
950
5000
5000
5000
1950
5000
5000
5000
5000
5000
5000
5000
5000
1500
5
5
5
95
5
5
5
5
95
5
5
5
5
5
95
50
150
5
95
5
5
5
195
5
5
5
5
5
5
5
5
15
SPIKING
'rom Spiking Standard
Spike(uL) cone combined
^01(1 00ml)
1000
1000
1000
1000
1000
1000
1000
1000
1000
1000
1000
1000
1000
1000
1000
1000
1000
1000
1000
1000
1000
1000
1000
1000
1000
1000
1000
1000
1000
1000
1000
1000
(ppb) total
so
50
50
950
50
50
50
50
950
50
50
50
50
50
950
500
1500
50
950
50
50
50
1950
50
50 ,
50
50
50
50
50
50
150
1000
1000
1000
2000
1000
2000
200
Element
Au
Ce
Li
P
Pd
Pt
S
Si
Sn
Sr
Orig Sid
(ppm)
1000
1000
1000
1000
130C
1000
1000
10000
1000
1000
Spike(uL)
Fvol{100
140
30
70
100
160
~CO
350
350
20
5
cone
(Ppb)
1400
300
700
1000
150U
joob
35CJ
35000
200
50
10OOuL of the Spiking Standard gives the listed cone, of the above elements.
Spiking Standard 2-110-3
Spiked by;
Predigestion-
Postdigestion-
- &
(J /CD
77
-------
PAGE 1 OF 2
,. ,. . , „_. 4
TRIANGLE LABORATORIES, INC.
Transfer Chain-of -Custody Form
Project
39568-A
Transfer From: IWL To: IA I
Released by:
Accepted by:
MILES. ID. .......
39568-A -
39568-A -000
39568-A -001
39568-A -002
39568-A -003
39568-A -004
39568-A -005
39568-A -006
39568-A -007
39568-A -008
39568-A -009
39568-A -010
39568-A -Oil
39568-A -012
39568-A -013
39568-A -014
39568-A -015
39568-A -016
39568-A -017
39568-A -018
39568-A -019
39568-A -020
39568-A -021
39568-A -022
39568-A -023
39568-A -024
39568-A -025
39568-A -026
39568-A -027
39568-A -028
Initials . ,
D^-
TLI No ....
OPR
TLI Blank
146-4-1A
146-4-1B
146-4-1C
146-4-1D
146-4-1E
146-4-1F
146-4-16A
146-4-16B
146-4-16C
146-4-16D
146-4-13
146-4-16E
146-4-16F
146-4-17A
146-4-18A
146-4-18B
146-4-18C
146-4-18D
146-4-18E
146-4-18F
146-4-20A
146-4-20B
146-4-20C
146-4-20D
146-4-20E
146-4-20F
146-26-1
146-26-2
Date Time
IV /At/ 1C, |i .^
Gust. Id
OPR
Method Blank
M29-1-A-AR2
M29-1-A-FH3
M29-1-A-BH4
M29-1-A-5A
M29-1-A-5B
M29-1-A-5C
M29-13-I-F1
M29 -13- I -BH4 -FILTRATE
M29-13-I-FH3
M29-13-I-BH4
M29-13-I-SA
M29-13-I-5B
M29-13-I-5C
M29-13-I-F1
M29-14-I-F1
M29-14-I-FH3
M29-14-I-BH4
M29-14-I-5A
M29-14-I-5B
M29-14-I-5C
M29-15-I-F1
M29-15-I-FH3
M29-15-I-BH4
M29-15-I-5A
M29-15-I-5B
M29-15-I-5C
M29-1-A-F1=BEAKER #102
M29-13-I-AR2=BEAKER #131
. _. . Y-Ft-rTir' ITS air 11 /n-i /QA\ __j_
Additional comments or instructions:
-------
PAGE 2 OF 2
TRIANGLE LABORATORIES, INC.
Transfer Chain-of-Custody Form
Project 39568-A
Transfer From: IWL To: IA I
Initials. . Date Time. . .
,^V?A ,« A* /"»/
Released by:
Accepted by:
U/ 2V
ll:
MILES.ID,
39568-A
395S8-A
39568-A
39568-A
-029
-030
-031
-032
TLI No Oust. Id.
146-26-3
146-50-1
LCS
Digestions
M29-14-I-AR2-BEAKER #136
M29-15-I-AR2 Beaker 140
LCS
Additional digestions
Additional comments or instructions:
-XfrCOC (Rev 11/01/94)--+
79
-------
PAGE 1 OF 5
• 1
TRIANGLE LABORATORIES, INC.
Transfer Chain-of -Custody Form
Pro j ect 3
Transfer From: IWLM
Released by:
Initials . .
Accepted by: U'^n
MILES . ID
39568-
39568-
39568-
39568-
39568-
39568-
39568-
39568-
39568-
39568-
39568-
39568-
39568-
39568-
39568-
39568-
39568-
39568-
39568-
39568-
39568-
39568-
39568-
39568-
39568-
39568-
39568-
39568-
39568-
39568-
-000
-001
-002
-003
-004
-005
-006
-007
-008
-009
-010
-Oil
-012
-013
-014
-015
-016
-017
-018
-019
-020
-021
-022
-023
-024
-025
-026
-027
-028
-029
TLI No
TLI Blank
146-4-2A
146-4-2B
146-4-2C
146-4-2D
146-4-2E
146-4-2F
146-4-2G
•146-4-3A
146-4-3B
146-4-3C
146-4-3D
146-4-3E
146-4-3F
146-4-3G
146-4-3H
146-4-4A
146-4-4B
146-4-4C
146-4-4D
146-4-4E
146-4-4F
146-4-4G
146-4-5A
146-4-5B
146-4-5C
146-4-5D
146-4-51
146-4-5F
146-4-5G
9568
To: IA I
Date Time . . .
\v I&J5L Ji= J^T
__»._...-. — — _.— _ — -.«-._-*-._-. ___».„___», ,n™___«._™m^
Gust .Id
Method Blank
M29-1-B-F1
M29-1-B-AR2
M29-1-B-FH3
M29-1-B-BH4
M29-1-B-5A
M29-1-B-5B
M29-1-B-5C
M29-2-A-F1
M29-2-A-AR2
M29-2-A-FH3
M29-2-A-BH4
M29-2-A-BH4
M29-2-A-5A
M29-2-A-5B
M29-2-A-5C
M29-2-B-F1
M29-2-B-AR2
M29-2-B-FH3
M29-2-B-BH4
M29-2-B-5A
M29-2-B-5B
M29-2-B-5C
M29-3-A-F1
M29-3-A-AR2
M29-3-A-FH3
M29-3-A-BH4
M29-3-A-5A
M29-3'-A-5B
M29-3-A-5C
Y-Fr-rnr1 foair ^^/n^/QA^ -±.
Additional comments or instructions:
80
-------
PAGE 2 OF 5
, • J
TRIANGLE LABORATORIES, INC.
Transfer Chain-of-Custody Form
Project 3
Transfer From: IWLM
Released by:
Initials . .
m
Accepted by: 0X&-
__»-_»._-.»._»._-. — — _.-*-,-.»
MILES . ID
39568-
39568-
39568-
39568-
39568-
39568-
39568-
39568-
39568-
39568-
39568-
39568-
39568-
39568-
' 39568-
39568-
39568-
39568-
39568-
39568-
39568-
39568-
39568-
39568-
39568-
39568-
39568-
39568-
39568-
39568-
-030
-031
-032
-033
-034
-035
-036
-037
-038
-039
-040
-041
-042
-043
-044
-045
-046
-047
-048
-049
-050
-051
-052 •
-053
-054
-055
-056
-057
-058
-059
TLI No
146-4-6A
146-4-6B
146-4-6C
146-4-6D
146-4-6E
146-4-6F
146-4-6G
146-4-8A
. 146-4-8B
146-4-8C
146-4-8D
146-4-8E
146-4-8F
146-4-8G
146-4-8H
146-4-9A
146-4-9B
146-4-9C
146-4-9D
146-4-9E
146-4-9F
146-4-9G
146-4-9H
146-4-10A
146-4-10B
146-4-10C
146-4-10D
146-4-10E
146-4-10F
146-4-10G
9568
To: IA I
Date Time .
\\iQ5ify % -.l*>arn
,, / ~^ , — , - , ^ . ;»— " __ ,1-jr-ML
u / 4 j / it Hr ; / ,> g~£ f}6.$ iii'i-j>«
Cust .Id
M29-3-B-F1
M29-3-B-AR2
M29-3-B-FH3
M29-3-B-BH4
M29-3-B-5A
M29-3-B-5B
M29-3-B-5C
M29-5-F1
M29-5-AR2
M29-5-FH3
M29-5-BH4
M29-5-BH4
M29-5-5A
M29-5-5B
M29-5-5C
M29-6-F1
M29-6-AR2
M29-6-FH3
M29-6-BH4
M29-6-BH4
M29-6-5A
M29-6-5B
M29-6-5C
M29-7-F1
M29-7-AR2
M29-7-FH3
M29-7-BH4
M29-7-BH4
M29-7-5A
M29-7-5B
Y-F-rrnr fpe^r ^^/n^/QA^__J.
Additional comments or instructions:
81
-------
PAGE 3 OF 5
TRIANGLE LABORATORIES, INC.
Transfer Chain-of-Custody Form
Project
39568
Transfer From: IWLM To: IA I
Released by:
Accepted by:
MILES. ID
39568- -060
39568- -061
39568- -062
39568- -063
39568- -064
39568- -065
39568- -066
39568- -067
39568- -068
39568- -069
39568- -070
39568- -071
39568- -072
39568- -073
39568- -074
39568- -075
39568- -076
39568- -077
39568- -078
39568- -079
39568- -080
39568- -081
39568- -082 •
39568- -083
39568- -084
39568- -085
39568- -086
39568- -087
39568- -088
39568- -089
Initials . .
(5KU
04
TLI No
146-4-10H
146-4-11A
146-4-11B
146-4-11C
146-4-11D
146-4-11E
146-4-11F
146-4-11G
.146-4-12A
146-4-12B
146-4-12C
146-4-12D
146-4-12E
146-4-12F
146-4-12G
146-4-13A
146-4-13B
146-4-13C
146-4-13D
146-4-13E
146-4-13F
146-4-13G
146-4-14A
146-4-14B
146-4-14C
146-4-14D
146-4-14E
146-4-14F
146-4-14G
146-4-15A
Date Time . . .
II/&/W Z-.ldam
jL_/_n:/Ab i\: \r
Gust. Id .
M29-7-5C
M29-FB-F1
M29-FB-AR2
M29-FB-FH3
M29-FB-BH4
M29-FB-5A
M29-FB-5B
M29-FB-5C
M29-RB-F1
M29-RB-AR2
M29-RB-FH3
M29-RB-BH4
M29-RB-5A
M29-RB-5B
M29-RB-5C
M29-10-F1
M29-10-AR2
M29-10-FH3
M29-10-BH4
M29-10-5A
M29-10-5B
M29-10-5C
M29-11-F1
M29-11-AR2
M29-11-FH3
M29-11-BH4
M29-11-5A
M29-11-5B
M29-11-5C
M29-12-F1
"yfr-rnr /T3*air i i /m /QA\ 1
Additional comments or instructions:
82
-------
PAGE 4 OF 5
TRIANGLE LABORATORIES, INC.
Transfer Chain-of -Custody Form
Project
39568
Transfer From: IWLM To: IA I
Released by:
Initials . .
Date , Time
Accepted by: HTuV \\ /2_^T7°I& 1^: fS~
MILES . ID
39568-
39568-
39568-
39568-
39568-
39568-
39568-
39568-
39568-
39568-
39568-
39568-
39568-
39568-
39568-
39568-
39568-
39568-
39568-
39568-
39568-
39568-
39568-
39568-
39568-
39568-
39568-
39568-
39568-
39568-
-090
-091
-092
-093
-094
-095
-096
-097
-098
-099
-100
-101
-102
-103
-104
-105
-106
-107
-108
-109
-110
-111
-112
-113
-114
-115
-116
-117
-118
-119
TLI No
146-4-15B
146-4-15C
146-4-15D
146-4-15E
146-4-15F
146-4-15G
146-4-17A
146-4-17B
•146-4-17C
146-4-17D
146-4-17E
146-4-17F
146-4-17G
146-4-19A
146-4-19B
146-4-19C
146-4-19D
146-4-19E
146-4-19F
146-4-19G
146-4-21A
146-4-21B
146-4-21C
146-4-21D
146-4-21E
146-4-21F
146-4-21G
146-4-22A
146-4-22B
146-4-22C
Cust.Id
M29-12-AR2
M29-12-FH3
M29-12-BH4
M29-12-5A
M29-12-5B
M29-12-5C
M29-13-0-F1
M29-13-0-AR2
M29-13-0-FH3
M29-13-0-BH4
M29-13-0-5A
M29-13-0-5B
M29-13-0-5C
M29-14-0-F1
M29-14-0-AR2
M29-14-0-FH3
M29-14-0-BH4
M29-14-0-5A
M29-14-0-5B
M29-14-0-5C
M29-15-0-F1
M29-15-0-AR2
M29-15-0-FH3
M29-15-0-BH4
M29-15-0-5A
M29-15-0-5B
M29-15-0-5C
M29-16-F1
M29-16-AR2
M29-16-FH3
__ --if-F-K-rnr footr i i /m /QA\ ___,_
Additional comments or instructions:
83
-------
PAGE 5 OF 5
). — ___ _. _ _ 1
TRIANGLE LABORATORIES, INC.
Transfer Chain-of- Custody Form
Project 39568
Transfer Front: IWLM To: IA I
Initials. . Date Ti tn<=
Released by
$
6
/I/
35l°& t..&«m
Accepted by: fD/MT ^ I "2^1 ^C? |"^ : \S
MILES . ID
39568-
39568-
39568-
39568-
39568-
39568-
39568-
39568-
39568-
39568-
39568-
39568-
39568-
-120
-121
-122
-123
-124
-125
-126
-127
-128
-129
-130
-131
-132
TLI
146
146
146
146
No
-4-
-4-
-4-
_4_
146-4-
146-4-
146
146
•146
146
146
146
LCS
-4-
-4-
-4-
-4-
-4-
-4-
22D
22E
22F
22G
23A
23B
23C
23D
23E
23F
23G
23H
Gust
M29-
M29-
M29-
M29-
M29-
M29-
M29-
M29-
M29-
M29-
M29-
M29-
LCS
— — ___ _ ____„_ — ^
.Id.
16-BH4
16-5A
16-5B
16-5C
17 -ACETONE
17-0.1NHN03
17-HPLC
17-5%HN03/10%H202
17-KMN04
17-8NHC1
17 -FILTER
17 -FILTER
y-F-rrnr1 nsair 1 1 /ni /QA^ _-o.
Additional comments or instructions:
Q/t
-------
-------
* SEE SPIKE LOG
Spiking Standard Preparation
element Standard Orig, Std. Spike(uL) — cone
ID (ppm)
ftg
fts
W
M
3
3a
3e
Da
2a
Id
5o
Dr
-u
re
re
<
<
*g
Hg
tin
Ji
>b
Sb
Se
n
n
v
Zn
2-84-7
2-84-6
|_ 2-84-7
2-75-3
2-84-7
2-84-7
2-84-6
2-84-6
2-7S-7
2-84-6
2-84-6
2-84-6
•2-84-6
2-84-6
2-75-8
2-84-7
2-30-2
2-84-6
2-75-9
2.-S4-6
2'-84-6
2-84-7-
2-80-1 •
2-84-6
2-84-6
2-84-6
2-34-6
2-34-6
2-84-6
2-84-6
2-84-6
100
100
100
10000
100
100
100
100
10000
100
100
100
100
100
10000
1000
10000
100
10000
100
100
100
10000
100
100
100
100
100
100
100
100
Fvol(IOOmt)
5000
5000
- 5000
950
'• 5000
5000
5000
5000
950
5000
5000
5000
5000
5000
950
5000
1500
5000
950
5000
5000
5000
1950
5000
5000
5000
5000
5000
5000
5000
5000
(ppm)
5
5
5
95
5
5
5
5
95
5
5
5
5
5
95
50
150
5
95
5
5
5
195
5
5
5
5
5
5
5
5
SPIKING
'rom Spiking Standard
Spike(ut) ' eon
-------
h
Cr
2-110-4
-V
IOO&
to
-4
$CQ
4-
w
d/
-.87
-------
* SEE SPIKE LOG
Spiking Standard Preparation
slemeni Standard Orig. SteJ. Spike(uL) cone
!D (ppm)
*9
&s
Al
V
3
3a
3*
3a
Sa
3d
Zo
Sr
2u
•e
:e
<
<
wig
v1g
vln
v1o
>Ja
4a
Mi
*b
Sb
Se
n
n
i/
In
Zn
2-100-5
2-100-4
2-1 00-5
2-105-7
2-1 00-5
L 2-100-5
2-100-4
2-1 00-4
2-105-8
2-1 00-4
2-100-4
2-100-4
2-1 00-4
2-100-4
2-1 05-9
2-100-5
2-1 08-7
2-100-4
2-106-1
2-* 00-4
2-100-4
2-100-5
2-108-6
2-1 00-4
2-1 00-4
2-100-4
2-1 00-4
2-100-4
2-1 00-4
2-100-4
2-1 00-4
2-1 06-5
100
100
100
10000
100
100
100
100
10000
100
100
100
100
100
10000
1000
10000
100
10000
100
100
100
10000
100
100
100
100 '
100
100
100
100
1000
Fvol{1 OOmL) (ppm)
5000
5000
5000
950
5000
5000
5000
5000
950
5000
5000
5000
5000
5000
950
5000
1500
5000
950
5000
5000
5000
1950
5000
5000
5000
5000
5000
5000
5000
5000
1500
5
5
5
95
5
5
5
5 -
95
5
5
5
5
5
95
L_ 50
150
5
95
5
5
5"
195
5
5
5
5
5
5
5
5
15
SPIKING
'ram Spiking Standard
Spiko(uL) cone
=Vol(100ml)
1000
1000
1000
1000
1000
1000
1000
1000
1000
1000
1000
1000
1000
1000
1000
1000
1000
1000
1000
1000
1000
1000
1000
1000
1000
1000
1000
1000
1000
1000
1000
1000
(ppb)
50
so
50
950
50
50
50
50
950
50
50
50
50
50
950
500
1500
50
950
50
50
50
1950
50
50
50
50
50
50
50
50
150
combined
total
1000
1000
1000
2000
1000
2000
200
"Spike seperately
Element Orig Std Spike(uL) cone
(ppm) Fvol(100 (ppb)
Au
Ca
Li
P
Pd
Pt
S
Sf
Sn
Sr
1000
1000
1000
1000
1000
1000
1000
10000
1000
1000
140
30
70
100
160
300
350
350
20
5
1400
300
700
1000
1600
3000
3500
35000
200
50
10OOuL of the Spiking Standard gives the listed cone, of the above elements.
Spiking Standard 2-110-4
Spiked by:
Predigestion-
Postdigestion-
-------
--.amis
Fri 11-22-5* 05:35:0'? fr.
Saipie Sse
Fiig nethoa Oste Tiis DpIO Typi fioce
1
2
3
4
5
7
8
9
10
11
12
13
34
15
11
18
20
21
22
23
25
26
27
29
30
31
NDl-Blii*
S7D3
STD3
CHECK 10
ICV/CCV
ivt/CCB
ICSAB
39568A r,S
3956BA LCS
i46-4-iH3i
146-4-iftsC ?i?5
146-4-iftEi; L
146-4-16A8CD
146-4-16ABCD DA
146-4-20A&
ICV/CCV
ICB/CCB
ICSftS
3%181/C 88
39618B/C LCS
146-4-isABCD XI 00
146-4-16A8CD Dft XI 00
i46-4-I8sBC
ICV/CCV
ICS/CCB
ICSfiB
• 112296
112296
112296
112296
112296
112296
112296
11229o
112296
112296
112296
112256
112296
112296
112296
112296
112296
112296
1122%
112296
112296
112296
112296
ii22?6
112296
112296
TRIANSL2
TRIAK6L2
TRIANSL2
TRIAWL2
7RIAWL2
7SIAWGL2
TRIAM6L2
TRIfiK6L2
7RIAH6L2
7RIAKSL2
7RIAH6L2
7RISH8L2
7RIftK6L2
7RIAHSL2
TRIAK6L2
TRIAH6L2
7RIANSL2
7RIAN6L2
7RIAH612
7RIANSL2
7RIAN6L2
7RIAK6L2
7RIAKSL2
7RIftN'SL2
7RIANGL2
7RIAK6L2
11/22/96
11/22/96
li/22/;6
ll/22/%
ll/22/?o
11/22/96
11/22/96
11/22/96
11/22/96
11/22/96
11/22/96
11/22/96
11/22/96
11/22/96
11/22/96
11/22/96
11/22/96
11/22/96
11/22/96
11/22/96
11/22/96
11/22/96
11/22/56
11/22/96
11/22/96
11/22/96
09:
Of;
09:
09:
10;
10:
10:
11:
11:
11:
11:
11:
11:
11:
12:
12:
12:
12:
13:
13:
14:
14:
15:
15:
15:
15:
•33
a
;i9
5s
;01
',12
17
12
17
32
17
'42
47
52
02
07
23
29
37
42
50
55
17
29
40
50
OSH
DKK
DKH
MH
DKH
DKH
DKH
DKH
DKH
SKH
DKH
DKH
DKH
DKK
DKH
DKH
DKH
DKK
DKK
DKH
m
DKH
DKH
DKH
X
X
1
9
fl
S
9
5
S
5
S
S
s
s
s
Q
S
i
S
s
s
s
5
n
«
C
s
IK
IK
cc-*c
COKC
Cu'iC
CChC
COKC
CORC
CCKC
CONC
C3KC
COKC
COKC~]
COKC 1
COKC
COKC
COKC
CORCl
CDHC J
COKC x^
COKC •"
cose
_£Mi>3l
cose
COKC
COKC
-------
auiJtarv
•us
uou<
^
3
4
;
r.
;
!
*•
10
i«.
.3
;4
i v
lo
1 1
18
i /
i'v
21
22
23
-*
25
2c
27
28
25
30
Si
32
33
34
35
f •
00
37
38
39
40
41
42
43
4*»
^5
46
43
49
- - - . _ . . . . t
S7L.i-ii.AH!'.
iT[<3
SI;--!
C«i> I",
572-i-suANK
i~';l
37D3
CitvK t'j
icv/;;cv
ICs/vCd
ICSA6
3^568 ^S
3lr5sS iCS
Ko-4-2A8CD
l»o---.A6Ci; PCS
Uo-i-2A8CD I
l4o-4-3ASCOE
14o-<2-3ASCDE DA
ii6-4-4ft6Ci>
146-4-5ABCD
iaj.-i-oA&CD
I '-I ' • /*.».. j
Itv.'U'
ICS/CCa
14o-4-3S8CPE
i4s-4-9A8COE
140-4-10ABCDE
146-4-I3A8CD
146-4-14ABCD
146-4-iSABCO '
146-4-17A6CD
I46-4-19A8CO
146-4-21A8CD
ICV/CCV
ICB/CCB
146-4-1 1A8COE
146-4-12A8CE
l4o-4-i20
146-4-22A8CDE
i4s-4-23ABD6K
» . i ^7^
lifl-a-ijC
146-4-2ASCO
146-4-2ABCD FOS
2-11C-4 iCCui/lOais
ICV/CCV
IC3/CC8
ICSSi
• •'-•
iiii''6
1126%
ii26-o
112c'%
1126%
ii2e%
il2s>9s
lliB%
1126%
iliD"%
1125%
1 1 40 *5
. i ^ «
ili5?C
112'0%
1126%
112696
1126%
1126%
112o96
ii269o
112o96
11 2696
1126%
1126%"
11269o
112696
112696
112696
11269o
112696
112696
112696
1126%
112696
112696
112696
112696
112696
H2c9c
112696
1126%
112870
1126%
H269o
i!2o%
112:-%
7:r"-1"l"
i nlASoLi
TRIhilGL2
TR!fi«6L2
TSI4»(6L2
TRlSf»SL2
TSIA«SL2
ISIANGL:
TRIA»uL2
TR1AH6L2
7RIAMSL2
TfliANiJs.2
TRI?ri i
OKH ,
OKH
OUri
OKH
OKrt
DKH
DKH
OKH
OKH
DKH
OKK
DKH
OKH
OKH
DKH
OKH
OKH ,
OKH J
OKH
OKH :
OKH
OKH ;
OKH
OKH i
OKH .
OKH J
DXK ,
OKH :
DKK ,
OKH :
OKH
DKH i
OKH
OKH J
OKH J
OKH ,
' IF, ~
IS
* I?
; coiii
. C3aC
IR
* IR
i COiiC
• COiit
; caac
; COHC
> COiiC
cosc
C3f!C
COK.
CONC
COttC
COnC
coxc
COHC
CONC
co;ic
cose
•^ f> y *
vuftL
COE
COKC
COXC
5 COMC
COKC
5 CONC
CONC
' CONC
COM
i COW
i COHC
3 CONC
; CONC
; COE
COHC
; COftt
CCHC
« KM1.M "
; iO?a-
C8SC,
5 COHC.
cose
*-*•*,!!•
ttiHt
Cft ,./,
vl**^
0
-------
PAGE 1 OF 3
TRIANGLE LABORATORIES, INC. |
Sample Preparation Tracking 4 Management Form f
Client: Pacific Environmental Services (PSS03> |
1
| Project: 39568A
I
1 Method:
| Solvent/Acids {):
fj(f'/0
Sample Information
Extraction Date: It ljLQrfv>
Lot:
0
i i
| I TLI
| Samplej SAMPLE ID
|# crd|
CLIENT
SAMPLE ID
I I I
| Sample [Final |
]Wgt lfio\\Volume| / /_
I 9 A ml A ml
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Method Blank
|A | 146-4-1A ,
|OQ1
M29-1-A-AR2
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|002
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|A | 146-4-1C
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|A | 146-4-1D
|004 I . ... ,,
|A
| 005
146-4-iE
|A | 146-4-iF
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M29-1-A-5C |
|A | 146-4-16A JbCA j. "Q |
|007 ) t^Kf- $Je" 3* f M29-13-I-F1 I' ^
|A | 146-4-16B
1008 | M29-13-I-BH4-FILTRRTE
|A | 146-4-16C
(009 |
M29-13-I-FH3
|A | 146-4-16D
1010
5 1 /flO
|A | 146-4-13
(Oil |
H29-13-I-5A
-#-
-REV V/26/93 JPSTMF T5—*
91
-------
PAGE 3 OF 3
I Project: 39S68A
TBIRNGUi WBQRATORIES, INC.
Sample Preparation Tracking & Management Form
Client: Pacific Environmental Services (PES03)
Sample Information
Method:
Solvent/Acids () :
j*zr
Extraction Date:
1 I
| ' I TLI /
| Sample | SAMPLE W 1 CLIENT
|# erd| / SAMPLE ID
1
111
| Sample | Final | |
| Heft / -toltoolume | _ / _ / _ | _ / _ / _ j _ / _ /
| g ral ml | II
_ / _ / _ | _ / _ / _ j _ / _ / _ j _ / _ /
|A | 146-4-20F
1026 '
M29-1S-I-5C
11
5 l /o6i
1
|A
]027
146-26-1
M29-1-A-F1=BEAK£R #102
A | 146-26-2
028 I M29-13-I-AR2=BEAKBR #131
|A I 146-26-3
1029 I M29-14-I-AR2=BEAKER #136
|A | 146-50-1
|030 | M29-15-I-AR2 Beaker 140
w
|A | LCS
|031
-,
LCS
|A ] Digestions |
|032 | Additional digestions |
i
| Comments:
-REV 07/26/93 SPS1MP 7)-~*
92
-------
PAGE 1 OF 11
TRIANGLE LABORATORIES, INC. j
Sample Preparation Tracking & Management Form j
Client: Pacific Environmental Services (PESOS) \
\
| Projects 39568
| Method: /T 'V .
I Solvent/Acids (i : H\ JO
Sample Information
Extraction Date: , / /_
Lot: £ ' '
\
\ \ TLI /
| Sample] SAMPLE ID / CLIENT
|# crd| / SAMPLE ID
-!£/$-, i
| Sample! j Final
|Wgt //foijl Volume | / / | / /_
| g /mlJ ml 1 |
/ _ /
/ / | / / |
TLI Blank /??<6 / |
Method Blank |
I I
i/OO I
1
| 146-4-2B
|002
| | 146-4-2C
|003 |
M29-1-B-AR2 ]
I I
M29-1-B-FH |
M29-1-B-BH4
J
146-4-2E
146-4-2F
M29-i-B-5B
146-4-2G
I00/
|
M29-1-B-5C |
146-4-3A&C'
I I
I I
\ 146-4-3B
I /ffV 1
I I
\ \ 146-4-3C
|010 |
I I
M29-2-A-FH
| 146-4-30^^
I , I
146-4-3E
|012
I I
M29-2-A-BH4
Comments:
i
-REV 07/26/93 (PSTWF 71—+
93
-------
PAGE 2 OF 11
| TRIANGLE LABORATORIES, INC. |
| Sample Preparation Tracking & Management Form j
| Project: 39568 Client: Pacific Environmental Services (PES03) |
. Sample Information |
1 Method: IT I® Extraction Date: . / / _._ '7% IA *»UJi t^S" !
1 Solvent/Acids!): //-SO . / HtJD} Lot: <3/fa
r~ J *J
GfQ/tlbOkQ / \
iSamplel SAMPLE ID / CLIENT |Wgt //foljvolumtt| __/__/ | / / | / / 1 "hf /f,, * /~/ i / f I
!# crd| / SAMPLE ID | g /{«M "1 1 1 1 1 **'»*•' | | j
| /Nj 146-4-3F |
01///I /,// r/ 5 I— "K M29-2-A-5A 1 f\
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|017 | M29-2-B-AR2 )/
| | 146-4-4C j\
|Q18 | M29-2-B-FH/ |
| y^, | 146-4-4D I
(Qlii/ | i»/V \L~lL~F) ~& M29-2-B-BH4 | O
| X\| 146-4-4E |
1 XNl 146-4-4F | I
lOSft//! /i// »/ ///— 'X M29-2-B-5B | 1
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j | 146-4-5A&C' V |
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| Mtjl 146-4-5B | /
102^^/1 M29-3-A-AR2 )/
| j 146-4-SC /I
|Q2S j M29-3-A-FH3/ |
1
1 Comments :
I
i /*& i i i i illi^n^ i i i
ii i i i ' i i i
ii i 1.1 i- . • i i
ii i i i i " i i
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iii i i 1 > i
i / i i i ' i I i i i
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i / i i i i / i i i
\
-------
PAGE 3 OF 11
1
{ Sample E
| Project: 39568
1 Method: I*fl0 Extraction Da
1 Solvent/Acids tl : tl^®,/ / t/AJ&a Lot: £(&(>
«. + *~ I __+ .
| TLI / 1 Sample
(Sample SAMPLE ID / CLIBKT |Wgt //ol
|| crd / SAMPLE ID | g /fully
| x«v 146-4-5D |
( si 146-4-5E |
| Sj\ 146-4-5F |
lOZft-' l^ttf^-SP" ' -^ H29-3-A-5B |
| x- 146-4-SG |
!•» w^Stt3>"»--^l'
| ($) 146-4-6B | \ £
|03JL M29-3-B-AR2 | /
| | 146-4-6C /
|032 | M29-3-B-FH3/
| yj\ | 14S-4-6D |
l"4c^ 1 ii// U / 7v A M29-3-B-BH4 | ,3
| /- | 146-4-6E I
I03C^ l*k,~*f~(f£ b M29-3-B-5A | ,5"
| ,» 146-4-6F | .
| _. | 146-4-6G | I
| | 146-4-8AfcC/ \|
| V ' 1 146-4-8B j/
|038 | M29-5-AR2/
1
1 Comments :
1
1
TRIANGLE LABORATORIES, INC. |
reparation Tracking & Management Form |
Client: Pacific Environmental Services CPSS03) |
S^irtple Information j
$$//fjpQ&& f 1
*
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Volume) / / | / / | / / |_ 3^/4^1 / / 1 / / 1
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95
-------
PAGE 4 OF 11
Sample {
Project: 39568
; Method: 'T / Extraction Da
i Solvent/Acids (): rf-^^t/ 1 H&'O'Z Lot: 31 ((><•
>• J -— '
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| | TLI / | Sample
1 Saraple] SAMPLE ID / CLIENT |Hgt / ao'.
] # ord / SAMPLE ID j g / tnlj
\ | 146-4-8C 1
|039 M29-5-FH3 | (^&Yk>
| | 146-4-8D^{J \ |
/v^i l^(f~ tf~$D¥£ O \
| | 146-4-8E [/
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| -.| 14S-4-BG !
|043f// |l/Y t/«-jP/?- /J M29-5-5B [
| - | 146-4-8H |
l°4£y 1 /v/£,-l/-F^ 7) H29'5*50 1 ^
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! J ^Ijl 146-4-9B | \
(04T5-' | ^529-6-AR2 | / S
| j 146-4-9C | /
|047 | M29-6-FH3"/
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1 /-si 146-4-9F !
1051(^1 .,/, (L_Q [? T) M29-6-5A t Q
\ S* | 146-4-9G | 1
>*/ \\4(f—^-^& "& *-^
I
1 Comments :
1
I
TRIANGLE LABORATORIES , INC. j
'reparation Tracking & Management Form |
Client: Pacific Environmental Services (PES03) |
Sample Information |
^ A . / / Iffa f I
"/" * * * * +~ * ' *
| Final | || ^l/l&Cfflfi^' |
^| Volume 1 / / | / / | / / | Jjfrfa, | / / | / / 1
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96
-------
PAGE 5 OF 11
I
| Project: 39568
TRIANGLE LABORATORIES, INC.
Sample Preparation Tracking & Management Form
Client: Pacific Environmental Services (PBS03!
Method: 7<#0
Solvent/Acids 0:
Sample Information
Extraction Date: / : /
r i TLI /
|Sample| SAMPLE ID / CLIENT
|# ord| / SAMPLE ID
\
[Wgt //VoltfVolume| /_
g H ml A ml
146-4-9H
111
M29"6"5C
5
146-4-lOA^C-
|OS3
M29-7-F
146-4-10B
M29-7-AR2 I
| |
| 146-4-10C
loss
M29-7-FH3
146-4-10D£
146-4-10E
|057
M29-7-BH4
| |
Hki
| 146-4-10F
146-4-10G
| 146-4-10H
'• tf(t-i-torf
M29-7-
7-sc ' 5
I 146-4-llA^g^
1 1 1
| | 146-4-1IC
|063 . |
M29-FB-FH3
| /S. | 146-4-llD£"
M29-ra-BH4
Comments :
-REV 07/26/93 SPSTMF 7)--*
9?
-------
PAGE 6 OF 11
Project: 395S8
TSIAHGLE LABORATORIES, INC.
Sample Preparation Tracking & Management Form
Client: Pacific Environmental Services (PES03)
1 Method:
I solvent/Acids<):
Sample Information
Extraction Dace: _ / /
lO
| | TLI /
|Sample) SAMPLE ID / CLIENT
|# crd / SAMPLE ID
I
| Sample rj Final |
|Wgt /^ft>lJVolu«e|_
ml I
146-4-11E
I I
M29-FB-SA |
146-4-11F
I , I
I I I
146-4-11G
I / I
|Q69
| S^\ 146-4-12C
I I
i 5"
146-4-12D
i i
g i (ffv i
146-4-12E O
10^3) I ,,ft ,1 >-,£f> j>
I I
I /T\l 146-4-12F7)
l<"li/l ..,, ./
I I
M29-RB-SB
1
0^
146-4-126
M29-HB-SC
l
i
14S-4-13A/i(L'
|075
M29-10-F1
11
146-4-138
H29-10-AR2
14S-4-13C
[077
M29-10-FH3
I Comments:
-REV 07/26/93 (PSTMF 7)--+
98
-------
PAGE II OF 11
TRIANGLE LABORATORIES, INC. |
Sample Preparation Tracking & Management Form |
Client: Pacific Environmental Services SPES03! [
| Project: 3.9568
Method:
1 Solvent/Acids (): M. ^O.
t
Sample Information
Extraction Date: /_
tot: Sl(eQt
I I
I I TLI /
|Sample| SAMPLE ID / CLIENT
|# crd| / SAMPLE ID
I I I
| Sample ' (Final | | |
|Wgt //VoU Volume | / / | / / (_
g /ml/| ml | | |
|
1130
f
5
IDD '
1 AfiS^-
,-
©
1 |
| Comments:
-REV 07/26/93 (PSTMF ?)-
90
-------
PAGE 1 OF 1
| TRIAHSLE LABORATORIES, IHC. |
) Sample Preparation Tracking & Management Form |
| Project: 39568 Client: Pacific Environmental Services (PES03) )
1
1 Method: ff'fO Extraction Date:
I Solvene/AcidsS) : >/. SO ^/^Mfe Lot: 3/^OfS
*~ * + *
Sample Information |
///(pQfeQ ff \
j I < 1 1 i l£ 1 4&£*f> 714*-
ISamplel SAMPLE ID / CLIENT l»gt //VolVolume I //!//!//! 3k*jtE" | //!//)
|# crd| / SAMPLE ID | g X«V'l »1 1 1 i 1 1 1 1
UP?/) jAC (if) LCS | ^r \ /I
! 0 ! ',«-t'*a *« ! ^ !"
(5 '/«,"- •/-«";> /«££> ' i i >
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1 | 1%- ^f-^D N. jj I I
iXOJX* - -- -- JL-_-Jt- * - >.
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I 1 /y.£-\{-££> At?E> J ' \|/ ' ,
*>! ! \nl*fa\ \
i i ' i / ii
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11 II
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I
I Comments:
1
1 1 I 1 1 1 1
1 1 1 I I 1 1
1 1 1 1 i if
1 1 I 1 1 1
1 1 1 1 1 1 I
1 1 1 1 j 1 1 I
1 1 1 I 1 1 1
1 1 1 1 1 1 i
1 1 1 1 1 I f
1 1 i 1 1 1 F
li
F
!
1 i
-REV 07/26/93 (PSTMF 7)—*
too
-------
PAGE
MERCURY SPIKE LOG
DATE
PROJECT #
SAMPLE IDs
ORIGINAL
SPIKE
CONC. (Hg)
STANDARD *
WORKING
STANDARD
PREPARED
FROM
AMOUNT
SPIKE
SAMPLE
(PPB)
INITIALS
WITNESS
(
>m
i
CM
Ml
^BCMSD
t-
i
M/
JLDJ
/' AS
-IIP MS)
*/
qa\forms\hgspke.log (08/22/96)
101
-------
PAGE
MERCURY SPIKE LOG
DATE
PROJECT #
SAMPLE IDs
ORIGINAL
SPIKE
CONG. (Hg)
STANDARD #
WORKING
STANDARD
PREPARED
FROM
SPIKE
AMOUNT
(ml)
SPIKE
SAMPLE
(PPB)
INITIALS
WfTNESS
iCSi
.0- fcm
SrJL
~ /£>&<=
N
qa\forms\hgspke.log (08/22/96)
102
-------
fieoort Table: HA277
Sun 11-24-96 06:09:22 ?«
oace 1
Taole Naie: HA277 Auiosanipler Tyoe: TYPE IJA
Saiple Positions: 171/192 OC Positions: 13/19 I Sits: 2
Rinse Station location is racK -1, DOS. -1,
- —
Rack
Racks —
1 Type
Usage
i ftux. i.L) Sack- STD/6C/8LANK
£
3
4
5
—
Sell
i
2
...
Sets
Saaple
Sansple
Sanple
Saipie
Saroole Sets
Type
Normal
Nonal ^
Preparation
Uptake
Ho Samples Prep
Sack
?os
l
2
3
4
5
6
n,.
Rack
Pos
i
L.
3
4
5
6
'7
8
9
10
11
12
13
14
11
Row Col
i i
1 2
1 3
1 4
i 5
1 6
il6w) Saiples
(I6w) Samples
(16mm) Samples
(loins) Samples
,—
Prepare? Description
Ho 39566A
Ho 396168/C
Info —
Uptake?? Final
arse.
3 £ ifi 3 1 V H i fli 8
SIM
STD1-BLANK
ICSAB
CHECK LO
ICV/CCV
ICB/CCB
«Pos
13
'27
48
48
48
Left Analyses/Pos
10
1
1
i
i
Method IPos RacKl St
artPos
TRIANSL2 9 2 1
IRIAH6L2 12 2
Oil.
Set
-fiA-
-NA-
-NA-
-Nft-
-NA-
-NA-
Factor
i SUsad
2
1
3
1
4
4
*
Type
Standard 1*^0-^
Standard
OC Standard \-iO't
CC Standard
OC Standard |-"io-\a
QC Standard
10
P "
IP
.? ,
,19 Hot Used)
12
HOW Col
1 i
1 2
1 3
1 4
1 5
1 6
1 7
1 8
1 9
1 10
1 11
1 12
2 1
2 2
Saaple Name
395683 K82.
39568a.LCSl-^a,utiua,
146-4-1AEC
146-4-lftBC POS
ii6-4-!ABC L
146-4-16A8CD X100
146-4-16A6CO DA X100
146-4-18SSC
146-4-20A8C
39618S/C MB
3961S8/C LCS
146-54-1
146-54-1 0
146-54-2
Set
I
i
1
1
1
1
1
1
1
2
2
2
2
2
i SUsed
-HA-
-NA-
-NA-
-NA-
--KA-
-NA-
-NA-
-NA-
-NA-
-NA-
-HA-
-KA-
-NA-
-NA-
Type
Sa»pie
Sample
Saiple
Sarooie
Sample
Saiple
Sample
Sanple
Sample
Sample
Saiple
Sample
Sanple
Sanple
103
-------
•>naivsis xeport
Averaaes
Fri ii-22-96 05:25:59 PH
page 1
Method: TRIAN6L2 Saipie Name: STD1-8LANK Operator:
Run Tiie: 11/22/96 09:38 filename: 112296
Moae: IR Type: X Corr. Factor: 1,00000
UD ID.: Oust. Sup!. 10.: Cust, ID.:
tlems
Jnits
Avge
SDev
SR5D
ileis
units
Avge
SDev
SRSO
Elans
Jnits
ivge
SOev
«SD
tlens
<;niis
Avge
SOev
4850
£iei»s
units
Avge
SCev
*,RSD
U3IS
Units
Avgs
SDev
ifiSO
ftg328Q
count
.00018
,00004
21.5169
CaSi/5
count
,00036
.00001
i. 16236
Fe271i
count
. J001
. jGOOi
22.57S6
Na3302
count
.00766
.00027
3.o0982
1960-i
count
-.00748
.00053
7.1802
V_2924
count
-.00076
0
1.02557
A13082
count
.00304
.00007
2.4819
Ca2265
count
-.00009
.00007
75 ate /
/ 0 , ™»>_ii.
KJ664
count
I, 35642
.04121
i.?49i
Hi25i6
count
-.002&2
.00012
4.72411
1960-2
count
.00284
.00009
3.41715
2n20o2
count
-.00002
.00002
107.812
fts!890
count
-.00045
.00012
27.2679
Ce4186
count
-.00007
.00013
168.429
Lio/07
count
.04415
.000/4
i.697
P_2i49
count
-.00116
.00015
12.976o
Snl899
count
-.0009
.00001
1.40475
Si28Si
count
.0354
.00258
7,30962
B.2496
count
.2266
.01483
6.54722
CQ2286
count
-.00023
.00001
b.53394
1102790
count
,00011
.00004
45,o341
2203-1 .
count
,0014
.0006
43.2517
Sr4215
count
,00027
0
2,01179
834934
count
,00059
.00001
1.94623
Cr2677
count
-.00017
.00001
6.74659
Hn2576
count
,00005
0
5.98416
2203-2
count
0
,00009
5582.06
T 13349
count
.00013
.00009
69.3895
Be3130
count
,00026
0
2,71558
Cu3247
count
.00395
.00003
,'1044
P0202C
count
.00002
,00005
187.427
8b2Q68
count
.00051
.0002
40.5744
T 11908
count
-.00049
.00003
7.24312
104
-------
Analysis Report
Hveraaes
m 11-22-96 35:25:59 Pti
page L
Method: TRIANGL2 Sasple Name: STDS Operator:
Run Time: 11/22/96 09:44 Filename: 112296
Mode: IR Type: X Corr. factor: 1.00000
Lab ID,: Gust. Snpl. ID.: Cust. ID.:
tleras Ag3280 A13082 Asl890 8J496 Ba4934 863130
Units count count count count count count
Avge ,34271 ,01566 .05172 .33067 .22622 .21018
SDe'v .00091 .00003 ,0006 ,00649 .00043 .00188
IRSD .26759 ,23481 1,16468 1.96327 .19084 ,8965
Eieis Ca3179 Cd2265 Ce4186 Co2286 Cr2677 Cu3247
Units count count count count count count
ftvg» ,01678 .76524 .0543^ ,077% .12542 ,14952
SOev ,00013 .00751 .00115 ,00067 ,00124 ,00057
°;RSD 1,13123 .9815 2.11499 ,37211 .99431 .38187
r8V;i4 ?»_.'6o4 L16/0--
count count count
, 'JuOv' i 16. ^08
1 A, A fl 1 A C 7 G i •*. i 7 G 3
,--'VvU"* ,"J~i\ji*j .vOC1-
1,59184 .39858 ,65055
count
,01755
Mri?57o rto2020
count count
,70014 .81119 .oSoiS
cleis
units
Avge
SDev
WSD
Eleins
Units
Avge
SDev
WSD
Eleis
Units
flvge
SDev
iRSO
Ha3502
count
,13115
.00003
.02934
1960-1
count
,25275
.00132
.52384
VJ924
count
.0295
.00018
,61922
Hi23lo
count
.30474 •
.00235
.77403
1960-2
count
.13893
.00155
1.12225
Zn2062
count
.07571
.00109
1,44987
P.2149
count
,0187
.00029
1.58205
Sni899
count
.11486
.00104
,91101
Si288i
count
.07541
.OOloo
2.21176
2203-i .
count
,15107
.00076
.59649
Sr4215
count
.64036
.00116
,18242
P62203
ii'yw-^'
count
,07548
.00094
1.25118
Ti3349
count
.8619
.00424
,49275
Sel%Q
862068
count
,10547
.00065
.62368
Til 908
count
,02fe05
.00069
2.64894
105
-------
Analysis Report Averages Fri 11-22-96 05:25:59 PM page 3
Method: TRIAMGL2 Sample Name: 3TD3 Operator: DKH
Run Tiie: 11/22/96 09:49 Filename: 112296
(loae: CONC Typi: Q Corr, Factor: 1.00000
Lao 10.: Cust, Sapi. 10.; Cust, 10.: 39568A
£le»s
Units
flvgs
SOev
IRSD
tisjis
units
Avgg
SDsv
iSSO
Elans
units
A«ge
". u 5 V
^RSO
£leis
Uni^s
ftvge
SDev
*RSO
Elems
Units
Avge
SOev
wso
tisms
Units
flvge
SDev
P30
Ag3280
ppo
998.9
0.748
.6756
Ca3179
ppb
1007,
2.896
.2877
-82714
PPD
- «W
i V W* V ,
i VJ . 0 3
1.064
rta3302
ppD
9978,
152.3
1.531
1960-1
ppo
995.3
15.11
1,518
V.2924
ppb
1003,
1.708
,1703
A13082
ppb
997.3
13.99
1.402
C02265
PP"
1005.
.2891
,0288
*_76oi
opm
10,10
.0*24
,4195
Ni2316
pDD
1007,
1.358
.1349
1960-2
PPD
9"54.3
2.641
.2656
In2062
ppb
1009.
5.726
.5675
AS1390
PPb
1002.
7.765
.7752
Ce4186
ppb
994.6
13.^7
1.405
L16707
poo
095.7
9.259
.93
?Ji4<5
PDD
998.5
8.958
.8971
Snl899
PPD
1003.
4.028
.4014
Si288i
ppb
541.2
8.941
1,652
8_2496
PPO
0938,?'
8.b5
.9215
Co2286
PPD
1004.
.61
,0608
MQ2790
ppD
99C . 5
1,311
1 •* * f\
2205-i
ppb
998J
10.17
1.018
Sr421S
ppb
992.4
6.585
.6635
Pb2203
ppb
998.3
4.097
.4104
8a4934
PPb
997.1
3.374
.8398
Cr2677
PPb
1004,
1,03
.1026
«n257o
opo
1002.
.7796
,0778
•2203-2
ppD
998,0
8.117
.3133
Ii3349
PPD
998.''
2.929
.2932
8el96Q
pob
994.6
6.747
.6783
883130
PPD
1004,
.2638
.0263
Cu3247
PPD
995.4
11.27
1.132
H02020
ppD
lOOo,
4.049
.4027
S&2068
pDD
1005.
5. 736
.3763
T11908
ppb
1018.
8.201
,8058
106
-------
Analysis Report Averages Fri 11-22-96 05:25:59 PM page 5
Method: TRIANGL2 Sample Name: 1CV/CCV Operator: DSH
Run Time: 11/22/96 10:01 Filename: 112296
Mods: CONC Type: 8 Corr, Factor: 1.00000
Lab ID,: Cust. Snpl. ID.: Cust. ID.: 39568A
ElSBS
Units
Avge
SOev
IRSO
tieffis
Units
Avge
SOev
IRSO
Eiems
uni;s
Avge
SOev
°;RSD
cleis
Units
Avge
SOev
IfiSO
El ems
Units
Avge
SDev
IRSD
Elems
Dniis
Avge
SDev
SRSO
Ag3280
ppb
497.e
1.41"
.2852
Ca3i?5
ppb
504.3
5.89b
1.169
F827U
ppO
502,;
9.94i
1.18
Na5302
ppD
4687.
62.11
1.325
1960-1
PPD
500.9
5,07
1.012
Ii5349
PPD
497.5
.o691
.1345
A13082
pp0
492.4
1.414
.2873
Cd2265
ppb
502.8
3,481
,6924
K.7664
Ppro
5.263
.0166
.3148
Ni2316
ppo
507.6
1,43
.2818
1960-2
PP°
499.9
4.221
.8443
111903
Ppo
506.1
5.726
1.151
AS1890
ppo
497.7
,9807
.1971
Ce4186
ppb
777.9
3.453
.4458
Lit>707
ppo
499,9
5.546
1,109
?_2149
ppb
500.7
1.974
.3942
Pb2203
ppo
498.6
3.839
T"*
. ; /
V.2924
pDO
502.3
1.714
.3413
B.2496
ppb
609.3
7.153
1.174
C02286
ppb
504.2
5.276
.6498
Mg279C
PPB
492.7
4.138
,3399
2203-1
Ppb
496.2
3.86
.778
Sel960
ppo
500.2
1.19
.2378
Zn2062
ppb"
504.0
4.775
.9474
8a4934
ppo
494.6
1.334
,3708
Cr2677
ppD
504.8
3.613
,7157
y A r "I ,'
rlniJ/S
ppb
500,5
2.t>59
,5313
.2203-2
ppb
499.8
7.468
1.494
Snl899
PPD
503.1
1.998
.3971
Si2S8i
ppb
310.9
12.5
4.02
883130
ppb
503.9
2.369
.5693
Cu3247
ppo
495,5
3.625
./ill
fio2020
ppo
307. c
i , ' i i
.542
Sb20o8
Ppb
509.5
2.361
.4634
Sr4215
ppc
498.0
1.065
n j 7 .
, Ai 00
10'
-------
Analysis Report,
Averages
Fri 11-22-96 05:25:59 PM page 6
Methoa: TRIflN6L2 Sample Naie: IC8/CCB Operator: DKH
Run Time: 11/22/96 10:06 Filename: 112296
flode: CONC Type: Q Corr. Factor: 1.00000
Lab ID.: Cost. Sipl. ID.: Cust. ID.: 39568ft
Elenis
Units
flvgs
SDev
*RSD
Eieras
Units
Avee
SDev
*>^_
ft!5082
ppb
1.047
.9329
89.11
'•/•i'^'Ks
'j U L i 0 J
ODD
-.3369
.0442
i3.ll
A_"to4
acin
.1441
.048°
•j 0 i 'fa
si 23 ID
pD3
'-.2580
.8139
31S.5
1960-2/
ppb/
71-290
Xi24
37.17
TS1908
ppD
36.55*
4,231
64.56
fts!890
m~ "
-3.171
1.313
41.41
Ce4l86
ppo
-.9834
2.453
249,5
L10707
3CB
,i^S2
,'Ja^i
55,i
P_2149
PCD
-2.4&2/
7. 515
30/4
/
Pb2203
ppb
.1741
2.462
1414
v_2924
ODD
.2771
.3666
132.3
B 2496
ppo
356,6
1.367
.5834
Co2286
PpD
.0888
.5522
396.5
' i1g2790
PpD
-1.311
1 • -'Uo /
;C7 Z /
w'U ' . - /
2203-1
/ppp
.3725
.3152
84. o5
Sel960
ppb
-.3978
.8889
223,5
Zn2062
ppb
-.1915
.533
278J
834934
ppp
' .1296
.0803
62
Cr2677
ppo
.2004
.5546
276,8
Mn257/
ppfc/
/C701
^1065
151.5
, 2203-2
ODD
' J751
3.78B
5045
SnlS99
ppb
1.131
1.913
169.2
Si2881
ppo
125.7
13.12
J&J&—
8e3130
ppo
.1119
.0476
42.49
CU3247 /
ppt) /
-.I/O
.0712
jfl .5
M02020
ppb
i.029
.5179
50,52
Sb2066
ppb
1,345
1.778
96.4
Sr4215
ppb
.1097
.0158
14.37
—— — "
105
-------
Analysis Report Averages fri 11-22-96 05:25:59 PM page 7
Method: TRIANGL2 -Sample Name: ICB/CC8 Operator: OKH
Run Time: 11/22/96 10:12 Filenaie: 112296
hoae: CONC Type: Q Corr. Factor: 1.00000
Lab ID,: Cusi, Sipl, ID.; Cust. ID.: 39S&8A
Eisus ftg3280 A13082 Asl890 1.24% 8a4934 6e5130
Units ppb ppb ppb ppb ppo ppb
ftvge -.2268 -3,51? -i.228 326.4 ,0198 -.0061
SOev .1529 3.745 .9087 2.65 .0525 .0149
IRSO 67.43 106.5 73,99 .8118 265.1 245.6
Eiems Ca3179 Cd2265 Ce4l86 Co2286 Cr2677 Cu3247
Units ppD ppb ppb ppo ppb ppb
ftvge .8798 -.4533 .6980 .0365 .0348 -,1117
SDev 1.779 ,143 2,445 .6834 .4937 .1555
IRSO 202,2 31.2 350.3 1884 1417 139.2
Fe27i4 K_76o4 Lio767 ?ig2790 Hn2576 Mc2020
ppo CDS opo ODD ppb ppo
Avge -3.018 .1314 ^D635 1.003 -.0545 .0928
SOev 10,15 ,051: .O'SS 5.061 ,0595 i
IRSO 126.5 40.04 i54.o 504,5 108.^ 1078
fia330I Ni231a P_2!49 2203-i 2203-1 3b2068
ppD ppD ppD ppb ppo ppo
-120,s -.5052 -0,278 -1.699 ,828o .66G4
21.s 1.512 5.103 2.426 1,77" 2.382
17,91 260,7 81.28 142.3 21*.6 360.7
Elems 1960-1 1960-2 ?b2203 Sei960 Sni899 5r4215
Units ppb ppo ppb ppb ppo ppo
Avge -1.151 .2669 -.0130 -.2052 .41% .0147
SOev .7932 1.541 .5005 ,795o 1,549 .0204
*RSD 68.93 577,2 3849 387.3 369.3 138,8
Eleus Ti3349 T1I908 VJ924 Zn2062 Si288i
Units ppb ppb ppb ppo ppb
Avge .0305 1.028 .2337 -,1885 10*.2
SOev .1281 3.171 .9018 .1467 12.96
IRSD 419.7 308.4 386 77.35 12.44
109
-------
Analysis Report Averages
Fri 11-22-96 05:25:59 PM
page 8
rteihod: TRIANG12 Sample Name: ICSAB Operator: DKH
Ron Time: 11/22/96 10:17 Filenaie: 112296
Mode: CONC Type: Q Corr, Factor: 1.00000
Lab ID.: Gust. S»pl. ID.:' Cust. ID.: 39568A
Eleis
Units
Avge
SDe'v
*RSD
Eiems
Units
Avge
SDev
IRSD
Eiems
Units
Avge
SDev
IRSD
Eieus
uni;s
Avgg
SDev
IRSD
tiens
Uniis
Avge
SDev
IRSD
Eleas
Units
Avge
SDev
WSD
Ag3280
ppD
542.2
.8323
.1555
Ca3179
ppD
466500.
4588
.9835
Fe27l4
ppb
i8i%u.
1009
.5517
Na5502
ppb
5967.
138.1
2,315
1960-1
PPD
525.9
i.5,75
2.991
Ti3349
DpD
504.2
1.461
.2898
ft!3082
opb
509900.
1672
.3279
Cd2265
ppD
483.9
4.175
,8626
K_76o4
ppiii
Qii.Si
.0811
.355o
N12316
ppo
'477.1
2.919
.6118
1960-2
ppb
507.4
10.31
2.032
T11908
ppD
504.6
18.46
3.659
Asl890
ppb
502.o
1.002
.1994
C64186
PPD
798.0
5.349
.6704
Li6707
ppD
65i. 3
5.679
.3716
•P.2149
DpD
583.3
20.36
3.576
Pb2203
ppo
506,o
8.316
1.641
VJ924
ppb
504.0
2.627
.5213
8J496
ppb
645.4
6.144
.9519
C02286
ppb
488.4
g.35
.7269
Mg2790
ppb
3ji/oo.
723.-
.1359
2203-1
PPD
508.7
6,925
1,361 '
' 3el960
ppb
513,5
2,009
.3912
Zn2062
ppo
445,2
7.791
1.75
Ba4934
ppb
517.8
1.904
.3677
Cr2677
ppb
492.9
4.3
,8724
Hn2576
ppb
300,0
3.383
.6507
- 2205-2
ppo
505.0
13.97
2.763
3(11899
ppb
502.4
1.368
.2723
S12S81
ppb
552.7
21.95
3,971
8e3130
ppb
504.3
3.596
.7131
Cu3247
ppb
554.5
4.227
.7623
H02020
ppb
495.5
4.772
,963
SP2068
ppfi
508.7
8.624
1.695
5r4215
pob
526.8
1.328
.252
HO
-------
Analysis Report Averages Fri 11-22-96 05:25:59 PH page 9
Method: TRIANGL2 Sample Name: 39568jf «82- Operator: OKH
Run Tiffle: 11/22/96 11:12 Filename: 112296
Mode: CQHC Type: S Corr. Factor: 1.00000
Lab ID.: Cust. Sipl, ID.: Cust, 10.: 39568ft
Elens Asl89Q Be3130 Cd2265 Co2286 Cr2677 Mn25?6
Units ppo ppo ppb ppo ppb ppo
fivge L-2.616 L.0296 L-,6eS2 L-.834S L-.0570 L.9443
SOev 1,663 .0556 ,1792 .4132 .2584 ,031
SRSD 63.56 120 26.93 49.51 453 3.918
EieiflS Ni23l6 Pb2203 Sb2068 3ei960
Uni;s ppb ppb ppb ppb
Avge L-2,697 1,7597 L.4017 L-.2565
SOev .2487 .8433 1.933 2.755
ISSD 9.222 111 432.5 1073
111
-------
Analysis Reoort
Overages
Fri 11-22-96 05:25:59 PH page 10
Method: TRIANSL2 Saiple Name: 39568/i LCS2. Operator: OKH
Run Time: 11/22/96 11:1? Filenane: 112296
Hode: CONC Type: S Corr. Factor: 1.00000
Lab ID.: Cust. Snipl. ID.: Cust. ID.: 39568ft
£le»s
Units
ftvge
SDe^
tRSD
fts!890
ppb
46.22
2,133
4.616
Be31JO
ppb
46.29
.1512
.3266
Cd2265
ppb
46.68
.2941
.6299
Co2286
ppb
47.15
.6016
1.276
Cr2677
ppb
47.88
.6274
1.51
Hn2576
ppb
47.68
.2721
.5707
Elems
Units
Avge
SDev
%RSu
N12316
ppb
45.63
.2815
.6169
Pb2203
ppb
48.04
1.909
3.975
Sb2068
ppb
49.21
1.42
2.885
Sel960
ppb
45.07
1.45
3.218
112
-------
Analysis fiaoort
Averages
Fri ii-22-96 05:25:59
page 11
Method: TRIANGL2 Sample Name: 146-4-lftBC Operator: OKH
Run Time: 11/22/96 11:32 Filename: 112296
rtoae: CONC Type: S Corr. Factor: 1.00000
Lab 10,: Cyst, Snipl. 10.: Cost, 10.: 39568ft
Eleis
Units
Avge
SDev
IfiSD
fls!890
ppb
50,02
5.641
11,28
Be3130
ppb
160.7
1.814
1,129
Cd2265
PPB
20.10
1.358
6.563
Co2286
ppD
209.3
4.446
2,124
Cr2677
PPb
306.7
2.968
.9677
Mn2576
ppb
427.9
3.139
.7335
Elens Hi2316 Pb2203 Sb2068 Sel960
Units ppb ppb ppb ppb
Avge 523.1 404.S 128.1 1058.
SOev 4.724 4.182 8.954 2.223
IRSD .9031 1.034 6.989 .2101
113
-------
Analysis Report Averages Fri 11-22-96 05:25:59 PN page 12
Method: TRIANGL2 Sample Name: 146-4-lftBC PCS Operator:
Run Time: 11/22/96 11:37 Filename: 112296
noae: CONC Type: S Corr. Factor: 1.00000
Lao ID.: Gust. Smpl. ID.: Gust. ID.: 39568A
Eiems
Units
Avge
SOev
IfiSD
ftsl89Q
ppt>
90.35
9.75
10.79
8e3130
ppb
203.2
2.085
1.026
Cd2265
PPD
62.00
1.501
2.421
Co2286
ppb
250. 9
5.796
2.31
Cr2677
ppb
355.4
4.699
1.322
Hn2576
ppd
473.4
2.74
.5788
tieas
Units
Avge
SOev
9»DCf'
4H,SD
N12316
pp0
567.2
5.894
1.039
PW203
ppb
443.9
7,o64
1.727
Sb2068
ppb
170.5
11.57
6.784
Sel960
ppb
1081.
6.802
.629
114
-------
Analysis Report
Averages
Fri 11-22-96 05:25:59 PM page 13
Method: TRIANGL2 Sansple Na»e: 146-4-1A8C L Operator; DKH
Run Time: 11/22/96 11:42 Filename: 112296
Node: CONG Type: S Corr. Factor: 1.00000
Lab ID.: Cust. Sropl. ID.: Cust. 10.: 39568ft
El ems
units
Avge
SOev
?-!Kn
'Biwu
fts!890
ppD
12.74
? Tin
0. V i 7
26,06
Be3130
PPb
37.45
.3594
.9597
Cd2265
ppb
4,544
.2466
5.427
C02286
pp0
48.96
1.536
3.137
Cr2677
ppo
83.79
1.311
1.564
Mn2576
ppb
92.84
,7768
.3366
Elens N12316 Pb2203 Sb2068 Sel960
Units ppb ppb ppb ppb
Avce 122,4 99,34 29.39 253.5
SDev .3389 2.137 2.423 2.994
IRSD .7264 2,151 8.243 1,181
115
-------
ftnaiysis Report averages Fri il-22-96 05:25:59 Pfj page 18
ilethoa: TRIANSL2 Sample Name: ICV/CCV Operator: DXH
Run Time: 11/22/96 12:07 Filename: 112296
(lode: CONG Type: 8 Corr, Factor: 1.00000
Lao ID.: Cust. Sfflol. ID.: Cust. ID.: 39568A
Elans
Units
Avge
SDev
1RSO
Eians
'JfliiS
Avgg
Osv
BSD
le-ii;
nils
VCS
ucV
ftSC-
EiaT.s
units
ftvos
SDeV
IRSC
Eleis
Units
Avge
SDev
IRSD
E18BS
Uniis
Avge
SDev
;
-------
Analysis Report Averages
fri 11-22-96 05:25:59 PM page 19
Helhofl: TRIftN6L2 Sainpie Name: IC8/CC8 Operator: OXH
Run Tine: il/22/96 12:14 filename: 112296
Hooe: CONC Type: Q Corr, Factor: 1,00000
tao ID,: Cusi. Smol. ID.: Cust. ID,: '39568A
ueis
Units
Avge
SOev
IRSO
Elens
Units
ftvge
SOev
IRSO
clems
-.inns
bens
units
Avge
SDev
IRSu
Eiens
Units
ftvge
SOev
IRSO
Eleas
Units
SDev
IRSO
Ag3280
ppB
,3007
,4167
138.6
Ca3179
PPD
Q525.5
91.61
28.15
AI3082 AS1890
ppb ppb
32.12 ,3770
11 r
Cd2265 Ce4l8o
ppb ppc
-.4208 1.484
.1507 .9217
35,82 62.1
8_2496
ppb
855.2
* 82,;
DDO
394
6. :<
169.3
1960-7 Pb2203
pplx ppb
4.170 -.5284
3,092 .8329
74,15 157,6
T11908 VJ924
PPD ppb
1.836 03,439
.7743 .807
42,18 23.47
Zn2062
ppb
.3945
.3171
80.38
Si2881
ppb
4150.
296.6
7,148
Sr4215
ppb
01.0%
.3154
28.78
117
-------
Analysis Report Averages
fri 11-22-96 05:25:59 Pf! page 20
Method: TRIftNGI.2 Sample Name: ICB/CC8 Operator; DKH
Run Tine: 11/22/96 12:23 Filename: 112296
Mode: CONG Type; 8 Core. Factor: 1.00000
Lab ID,: Cust. Snpl. ID.: Cust. 10.: 39568A
Eleus
Units
ftvge
SDev
tRSD
Eiems
Units
ftvge
SOev
IRSD
Elens
Units
Avge
SDev
IRSO
EISBIS
Units
Avge
SDev
IRSO
i less
Units
ftvge
SDev
IRSO
Elems
Units
flvge
SDev
IRSD
Ag3280
ppb
-.6414
.8845
137,9
Ca31?9
ppb
14,49
3.264
57.02
Fe2714
ppb
•10,62
6.891
64.37
Na3302
ppb
-194,4
240.1
123.5
1960-1
ppb
2.523
4.065
175
Ii3549
ppb
.0852
.0576
67.54
A15082
PPB
25.82
7.279
28.19
Cd2265
ppb
-.6042
.0939
15.55
K.7664
ppji
.17=55
.0526
29.35
Ni231o
opo
.3980
1.038
260.8
1960-2
PP°
-.6670
2.454
364.9
T11908
ppb
-1.551
2.884
185.9
Asi890
ppb
.7199
1.05
145.8
CS4186
ppb
.7085
1.243
175.5
L16707
PPb
.2542
.0924
36.37
P 2149
ppo
,9392
,3027
32,23
Pb2203
ppb
-1.40*
.201
14,32
VJ924
ppS
82.534
.7479
29.51
8_2496
ppb
781.4
80.61
10.32
Co228o
ppb
,0583
.047
122.3
Mg2790
PPB
-.5152
-^ •* , i
.iiOO
45 , 85
n r- f* ~ ^
2iUo-l
ppc
-2, Ik"
5.871
178.6
Sei960
ppb
JZSS
1.154
350.9
Zn20o2
ppb
-:0674
.2112
313.4
8a4934
-ppb
.0876
,0426
48.69
Cr2677
ppb
.5615
.0778
13.85
fln2576
ppc
.5403
.6006
118.2
^'5A"-'5
£i.Uu i.
ppo
-1.022
1.633
159.7
Snl899
ppb
1,582
.5717
36.14
Si 2881
ppb
2104.
223.5
10.62
8e3130
ppb
.0145
.0524
362.4
Cu3247
ppb
Q-2.028
.7741
38.16 -
i1o2020
ppb
,o755
.522o
47,92
362068
ppo
-.6017
.728
121
Sr42i5
PPb
,0570
.029
50.35
118
-------
analysis Report Averages rri il-22-96 05:25:59 PM page 21
rtethod: IRIANGL2 Saiple Naie: ICSAi Operator: OKH
Run Time: 11/22/96 12:29 Filename: 112296
MODS; CONC Type: 8 Corr, Factor: "l.00000
Lao 10.: Cust. Smpl. ID.: Cust. ID.: 39568A
Eiems Ag323G AI3082 Asl89Q 3_2496 Ba4934 Be3130
units ppD ppo ppo ppD ppo ppo
avgs 537.9 500200. 502.8 1.170. 520.9 499.6
5D=v ,5665 2978 8.332 68.66 3.227 4.079
?;RSO ,1055 ,5952 1.657 5.869 .6196 ,3163
tisas
Units ppfi ppD ppb ppb ppb ppb
Avge 452800. 4/8,2 792.7 482.1 ' 489,2 547,5
SDsv 4942 2.336 2,048 3.494 4,o49 6.176
iRSD 1.091 ,5513 ,2583 .7248 ,9504 i.i23
Elsffls Fe27i4 K_7664 U67G7 iig2790 Hn2S76 ?lo2020
Units
1SOSOO,
8S7.&
,4^09
Ha3302
ppb
5994,
112,4
1.875
1960-1
ppb
525.3
20,46
3,696
Ti3344
ppD
489, i
1.062
~~ ™ ^
.020*
. 0899
Ni?316
ppo
47i. >
2.711
.5722
1960-2
ODD
506 , 5
7.724
1.525
Til^OS
BpO
493, 7
is.ai
D51.3
3,312
,5849
P.2149
ppb
30^,3
7.057
1.235
?b2203
ppb
496.3
2.739
,551^
V.2924
ppb
502,9
3,365
527300.
192,5
.0365
2205-i
ppb
497.5
4.932
.9913
Sel960
ppo
512,7
i.981
,3864
Zfi2062
Ppb
441.2
8,371
V"'0 '.
3.261
,o263
2203-2
ppb
495,8
5,944
1,199
3nlS99
ppo
484.7
5,449
1.124
Si 2881
ppb
1881.
76,22
491,^
5.914
1.202
S b2068
PPD
507.3
4,029
,7941
Sr4215
ppb
521,9
2,137
.4094
tiSfflS
Units
Avge
SO ev
tieis
Jnijs
Avgs
SDsv
IF.SO ,2172 3.809 .6691 1,397 4,051
113
-------
Analysis ttepor:
Averaaes
fri 11-22-96 05:25:59 PM page 29
Method; TRIANGL2 Saiple Naie: ICV/CCV Operator: OKH
Run Time: 11/22/96 15:29 Fiienaie: 112296
(lode: CONC Type: Q Corr, Facior: • 1.00000
lab ID,: Cust. Sapl. ID.: Cust. ID,: 39568A
El ems
Units
Avge
SDev
WSD
Elems
units
Avge
SOev
IRSD
Eleus
Unus
Avge
SDev
IRSO
ElSlilS
Units
Avge
SDev
*osn
•ofwU
Elsiis
Units
Avge
SDev
IRSO
ileus
Units
Avge •
SDev
IRSO
Ag3280
pOD
496.5
2.767
.5573
Ca3i"9
PDD
81426.
348,!
24,47
re27i4
ppo
5ii.:
9.67^
1 . 883
Ha5302
ppb
4824.
46.55
.9651
1960-1
ppD
487.8
3.461
1.735
71334V
ppb
466.2
i.887
.3881
A13082
ppb
Q570.7
23.69
4.152
Cd2265
PpD
500.5
2.798
.5593
K_.7664
ppli)
3,i33
.0252
.4715
Ni23i6
ppo
505.7
2.706
.535
1960-2
PPD
49<5,3
5.457
i.093
111908
ppb
.1 Q7 ™
T ' ! , \l
13.75
2,765
AS1890
ppD
502.0
.4892
.0974
Ce4lS6
ppb
775.6
i.349
.1743
iio707
ppD
50; , 8
2,711
.5338
?_2149
ppb
509,5
5.661
i.iii
3b2203
ppo
489.0
5.051
.6239
VJ924
ppb
SOb.6
1,843
,3657
3_2496
ppo
368.6
9.552
2.592
Co22S6
ppD
498.7
3.043
,6101
?fg2790
PPD
SOj.'i
7.335
i.45i
2205-i
ppb
475.9
4.455
.94
S81960
ppD
495.4
5.774
1.165
Zn2062
Ppb
503.5
5.621
1.117
834934
PPD
498.2
2.975
.5971
Cr2677
ppo
503.0
2.636
.5241
i1n2576
ppD
»87 , •?
i . ?44
.3984
2203-2
ppb
496.5
6.691
1.348
Snl899
ppb
481.7
3.281
.681
Si 2881
ODD
1S59.
365.4
19.65
Be3130
PPO
502.5
2.466
.4907
Cu3247
ppb
488.4
4.601
,942
1102020
ppo
iui.i
.4558
.0909
882063
ppb
508.5
1.325
.2602
Sr4215
ppo
496.3
2.046
.4123
120
-------
Analysis Report Averages . Fri 11-22-96 05:25:59 PM page 30
Method: FRIANGL2 Sample Name: ICB/CC8 Operator: OKH
Run Tine: ll/22/% 15:40 - Filenaie: 112296
Mode: CONC . Type: Q Corr. Factor: 1,00000
lao 10,: Cust, Srapl. ID,: Cust. ID,: 39568A-
tleis
Units
Avge
SDev
*RSO
Eieais
units
Avgg
SDev
MSO
iieas
units
SDav
:;RSO
Eisis
Units
Avge
SDev
SR5D
Eiems
Units
Avge
SOev
•ifiSO
E13BS
units
Avge
SOev
IRSO
Ag3280
PPD
,0080
.3579
4448
Ca3l79
pp0
14.95
7.o58
51,21
Fe27i4
ppb
-17.05
3,425
20.0^
Na3302
opo
-95.39
54.29
35 . 95
1960-1
ppb
1,641
,6115
37.26
Ti334<3
ppb
.1635
.0222
13,57
(U3082
ppb
Q65.85
6.823
10.36
Cd2265
ODD
-.4358
,0i57
10.48
IL7604
m
.0591
27.58
Ni251*
PPO
-.1924
,&569
341.5
1960-2
ppb
-3.853
1.361
48.3
T11908
ODD
,5317
1,09
205
AS1B90
ppb
-.9782
1.42
145.2
Ce4186
ppo
-2.464
i.912
77,62
U&7C7
PCD
.055
21.09
P.21^
PpD
5.532
4,86o
91.27
Pb2203
ppp
.1991
.3661
435
V 2924
ppo
84,447
.4792
10,77
8J496
PPD
81.11
6.37
7.853
Co2286
ppo
.0860
.0356
41,38
iig2790
DDD
.'•"13°
523.3
2203-i
ppo
.5767
1,291
542.0
3el960
PpD
-2.023
1.103
Sa.52
Zn2062
ODD
,0511
.1406
275
B34934
ppb
,1115
.0301
27,01
Cr2677
ppb
.1369
.133
100,9
iifl2576
Ppb
"^'Mc"*!
755,9
2205-2
ppo
.1104
1. 382
1704
Snl899
ppo
1.076
.1576
14. o5
S12881
ppo
450.3
57,56
13,38
8e3130
ppb
,1649
.0568
34,43
Cu5247
ppp
6-3,797
,4159
10.95
;102020
ODD
.1328
42.79
3b2063
ppo
-1.588
2.231
140.5
Sr4215
pps
,0974
.0216
22.19
121
-------
analysis Report Averages Fri'11-22-96 05:25:59 ?M page 31
Hethoa: TRIANG12 Sample Najie: ICSftB Operator: OKH
Run Time: 11/22/96 15:50 Filename: 112296
Poae: CONC Type: 9 Corr. Factor: 1.00000
Lab ID,: Cust. Siimi. 10,: Cust, 10,: 39568A
El ens
units
Avge
SDev
IRSD
Eleros
Units
Avge
SDev
5RSu
ileus
unii3
Avos
SDsv
%R$D
iie«s
Jnus
Avce
SOev
wso
Eleas
Units
Avae
SDev
WSO
tieins
units
Avge
SOev
SRSD
flo328u
ppb
545.0
1.424
.2612
Ca31?9
ppb
459200,
4015
.8/4.5
?e-"u
opo
1535GU,
3Zi, i
,44b
NaiC-u'I
ppo
Q6094.
36.9
1 , 425
1960-i
PPD '
521.7
17,35
3.361
Ii33*«J
ppb
495.4
1.063
.2146
A13082
ppo
506600.
2617
.5561
td2265
ppb
483,8
2.oS9
.5557
«_7eb4
OpITi
322.31
.0734
.3438
Ni23io
ppD
478.9
3.888
.8119
1960-2
ppp
517.o
11.92
2.303
T11908
ppb
498,6
27.46
5.505
Asl890
PPD
510.0
1.104
.2165
C64136
ppb
'803.2
1.232
,153i
Lls707
PPD
o58.«
2.4C'S
.37S4
PJ140
bpb
578.9
15.13
2,614
Pb2203
PPD
501.7
5.241
1.045
V_2924
ppb
513.2
3.792
.7333
8_2496
ppD
390.2
6.381
1,636
C02266
ppb
487.1
2.996
.ol52
fig2790
ppo
534900,
199.0
.0373
2203-i
ppb
492. G
4.674
.95
Sel9oO
pps
519.0
3. 2
.6167
Zn2062
PP&
445.6
7.655
i.718
Ba4934
ppo
529.3
2.629
,4967
A _ .1 -- "• "T
h'ibl i
ppb
496.0
4,037
,.314
Iln257o
Ppo
"'0 ™
2.oi3
.1QTS
. -7^0
2205-2
Ppb
506.6
9.404
i.SSo
Snl899
ppD
485.1
3.352
,691
Si2881
PPD
662.2
6,668
1.01
3e3130
ppo
505.5
3.311
,7538
Cu3247
ppb
555.1
5.43
.«783
fio2020
OpD
iQ5,6
Z . o 4 o
1,082
3b20o8
PPD
508.5
i.025
.7924
Sr4215
ppD
533.2
i.609
.3013
-------
.1A279
i»lea 11-27-96 07:50:29 ?M
oacs l
Taole Mia: HA279 Autosampier Type: TYPE TJfi
Saisie Positions: lob/192 CO Positions: 15/15 I Sets: i
Rinse Station location is racn -1, pos. -i.
Usaae
itPos Left Anaivsss/Pos
i
i
->
«i
.
wC C?
ietJ
SOS
Pos
2
3
4
3
6
(L.
RaeK
HOS
i
,i
4
5
a
7
5
9
10
u
12
13
14
15
^ux. i
Sample
Saapia
Sajpis
•vdiiiDie
:ype
soni.ji
'"fsoa ratio
'.- p l a -\S
51
now Cfli
i 1
1 2
i 3
i 4
1 S
1 6
.19 sot
32
HOW CO i
i 1
i 2
1 3
i 4
1 5
1 6
i 7
i e
1 9
1 10
1 li
1 12
2 i
L 4
2 3
LJ MCX sTO/QC/SLANK
i. lofitni] Sastpiss
(loiMJ Samples
(ism) Saffioies
\loiilfflj SalTipleS
Prepare? Description
i>0 0'ijOO
n iflrC' —
ijota«ss2 final
parse.
Sample Name
STD5
STDi-BLANK
IC3A8
CHECK LO
ICV/CCV
ICB/CC8
Used)
Saipie Naae
39568 M8'l
39568 LCSX •s-^-v.S'
t46-4-2A8CO
146-4-2A6CO POS
146-4-2A6CO L
146-4-3A9COE
14o-4-5A8CO£ M
146-4-4A8CO
146-4-5A8CD
14o-4-6ASCD
146-4-3A6CDE
146-4-9ABCOE
i46-4-10A8COE
146-4-13A3CO
146-4-14ABCO
Oil.
Set
-NA-
-NA-
-NA-
-NA-
-NA-
-Nft-
Set
1
i. 1
i
1
1
1
i
1
1
1
i
1
1
1
1
flee
TRI
Factor
1 itUsed
2
\
2
1
4
4
t iUsed
-NA-
-NA-
-Nft-
-NA-
-NA-
-NA-
-MA-
-NA-
-NA-
-NA-
-Nft-
-NA-
-m-
-NA-
-NA-
15 10
22 1
48 I
48
40 1
noi] sPos Sacxj 5tar;?os
nitblZ 2o 2 i
Type
Standard 1-30-lvP
Standara
yC Standard \-3O-l3i
CC Standard
QC Standard i-'io-li.'P
QC Stanaara
Type
Saiple
Saioie
Sanple
Sample
Saipie
Saipie
Saapie
Sanpia
Saapia
Saiipie
Sanple
Saspls
Satnple
Sample
Saiple
.
n Cj
V*-'
123
-------
AutoSampier Report Table: HA279
Sac* <2
HOS Son Coi Sawie Name
Kea li-27-96 07:50:29 P«
Set it dUsea Type
oaae
,6 2
17 2
i8 2
19 2
20 2
21 2
22 2
23 2
24 2
25 5
26 3
(27. ..48
?05 HOW
11... 48
Rack Si
?OS KO'*
;.l... 48
Rack §5
?OS HOW
4
5
6
7
8
9
10
11
12
1
v
Not
Col
Not
Coi
Not
Coi
146-4-15A8CO
1 46-4-1 7ABCO
146-4-19A8CO
146-4-21A8CD
146-4-11A8COE
146-4-12A8Ct
146-4-120
146-4-22ABCOE
146-4-23A806H
146-4-25C
t empty }
Usedi
Sanpie Name
Used)
Sampia Na»e
Useo)
Sanoie fiaie
1 -NA-
1- -NA-
1 -NA-
1 -Nft-
i -NA-
1 -NA-
1 -ftA-
1 -hA-
i -HA-
1 -NA-
i -Nfi-
Sst -t -iUsed
Set i sUsea
Set 1 itUsed
Saaple
Saipie
Sample
Sampie
Saipie
Sample
Sample
Sample
Sample
Sainple
-HA-
lype
Type
Type
i,i...4S Hoc Useo)
124
-------
Analysis Report Averages Mea 11-27-96 05:43:09 PM page 6
method: TRIANG12 Sample Name: STD1-3LANX Operator:
Run lime: 11/26/96 12:36 • Filename: 112696
floae: IS fyoe: X Core, factor: i,00000
Lao ID.: Cust. Smpl. ID.: Cust. ID.:
Eisins Ag5280 A13Q82 fcl890 8J496 Ba4954 8e5130
Units count count count count count count
Avge .00011 ,00484 -.00067 .0026 ,00058 .00036
SDev .00024 .00003 ,00011 .00008 .00001 0
^sfiSD 207.555 ,78932 17,o642 3.12943 2,71006 i.13426
Elesis Ca3179 Cd2265' Ce4136 Co2286 Cr2677 Cu3247
Jniis count count count count count count
Avge .00009 0 -.00008 -.00034 -.00017 .00462
SDev 0 .00034 .00006 .00001 .00007 .00002
8.00426 4740.13 77.544 5.02352 40.5027 .4737:
Fe27l4 i\_?oo4 lio"G7 ng2790 ?in2576 302520
:oufH count couni count count ccun;
.00013 2.49353 ,C4?2S ,0001^ .OOOOc .OCJii
,OOCi&3 ,u4i/ .1)0086 -OOOOi 0 .OOuus
39.^534 i.7G278 1.7fc007 .5.7^355 i 0.200*
count coani; count count count ccun*
.OOoo -.00372 -.00169 .00208 .00022 .00071
.00055 ,000io .00005 .00053 .00017 .00012
4.90195 4,401o5 3.33712 lfr.2769 74.6672 17.5366
tifiiiis 1960-1 1960-2 Sni899 Sr4215 Ti33i9 T11906
Units count count couni count count count
Avge -.00965 .00415 -.0012 .00027 .OOOOS -,00071
SDev .00044 .00021 .00019 .00001 .00006 .00006
IRSO 4.58991 5.2658 16.366S 6.86009 78.5935 3.8237
[lens V_2924 Zn20o2 Si2B31
units count count count
Avge -.00084 -.00007 .03535
SOev .00001 .00001 .00065
IRSO 1.70044 20.3392 1.34354
12;!
-------
Analysis Report Averages
Wea il-27-96 05:43:09 Pfl page 7
Method: TRIANGL2 Sauple Name: STD3 Operator:
Run Time: 11/26/96 12:41 Filename: 112696
Hooe: IR Tyoe: X Corr. Factor: 1,00000
Lao ID.: Cust. SiDi. ID,: Oust. ID.:
Eleus
Units
fivce
SDev
mi)
El ens
Units
Avoe
SDev
IfiSD
Eiams
Unns
Avga
SDev
iRSO
lisas
units
AVQ =
Sfrev
$RSD
ElefflS
Jnits
Avae
SCev
SfiSD
tieis
Units
Avge
SDsv
SfiSD
Ag3280
count
,48749
.00142
.29251
Ca3179
count
.02^14
.00023
.96258
re27!4
count
.00477
.00006
1.35106
Na5502
count
.12457
.00175
1.40829
i°60-i
count
.54784
.002:5
.73314
v ?
-------
Analysis Report Averages (led 11-27-96 05:43:09 PM page 8
Method: TRIANGL2 Sample Name: STD3 • Operator:
Run Tine: 11/26/96 12:4? - Filename: 112696
Mode: CONC Type: 0 Corr, Factor: 1.00000
Lab ID.: Cust. Supl. ID,: Cust. ID.: 39568
tienis Ag3280 A13082 fis!S90 8_2496 8a4934 6e3130
Units ppb ppo ppc ppb DDD ppc
Avge 992.6 990.9 992.0 992.7 991,7 991.1
SDev 16,73 26.18 18.05 15.56 16.96 11.06
*fiSD i.aSS 2.642 1.S19 1.563 1,71 1.176
Eieins Ca317> Cd2265 Ce4186 Co2286 Cr2677 Cu32*7
ufii'.s ODD • ppo opo ppo ppb pps
Hvge 995,9 992.7 ?7o,3 993.1 992.7 990.9
SDev 10,73 10.94 14.41 10.o5 11.21 21.4*
\m 1,085 1.102 i.475 1.072 1,13 2.16*
units ppo pprn PDD ppb DPP ppo
Avce 997,3 L0.07 °^i," 99i.i ^i.5 992. •>
SDev 15.98 .096 25.71 15.61 11,08 15,2
•1RSD 1,602 .9537 2.553 1.369 i.173 1.531
Eiess Na3302 NJ2316 ?_214? 2203-1 2205-2 5b20o3
Uniis ppb ppo ppD ppo ppo ppo
ftvge 1006C. 993,9 1001. 993.0 990.6 992,-
SDev 105,i 10,97 9.285 10.79 7.&31 12.5
1RSD 1.052 1,104 ,9274 1.087 .7703 1.24
tlsis 1960-i 1960-2 S(U899 Sr4'2l5 715349 T11908
Uniis ppb ppb ppo ppo ppb poo
ftvce 99o,3 998,2 992.3 5S9.i 991.2 ?90,7
SDsv 19.04 14.37 14.56 15.6 13.29 i2.0o
IRSD 1,972 1.489 1.447 i.577 1.341 1,2:8
ilsK v_2924 Zn2062 Si288l P62203 Sel9oO
Units ppo DDD ppo ppb ppo
Avge <:?92,0 992." i87,3 9?1,4 997,5
SDev 13.56 11.08 10.74 3.258 16.15
%8SD 1.567 1.116 2,202 .8329 1.617
12'
-------
Analysis seport Averages flea 11-27-96 05:43:09 PM page
fletnoa: MANGL2 Sample name: ICV/CCV Operator: OKH
Run Tine: 11/26/96 i2:57 Filename: 112696
floae: CONC Type: Q Corr. factor: 1.00000
Lao ID,: Cust. Snpi. ID.: Cust, 10.; 39568
lenis Ag3230 A130S2 Asi890 8_2496 6a4934 8e3130
10
Units
fivge
SDev
WSD
tieras
Units
fivge
SOev
IRSD
£l3«S
•jr.iis
A V'"10
-v
SO 3v
Ei5i» =
Jfii;s
4vo£
SDev
%R5&
tleiiis
Uniis
Avge
SDev
IRSD
£ie»s
Uniis
Avge
SDev
%RSO
ppb
509.2
.8185
,1607
Ca3179
ppo
509.8
6.359
i.244
r~e27Li
3DD
- | /
i- , 4-
^m
• ODD
4829.
99. 5o
2,0o2
1960-1
ppo
50o.3
.7222
.1425
71334=
ppb
503.0
2.3
.4572
ppb
505,0
3.491
,6905
Cd2265
pD0
505.7
5.7S5
,7485
!<_'oo4
DOB
-. . •-(<
' i" '
r)'"'3'o
ppc
510.4
3.97.3
.7784
1960-2
ppo
j06,8
5.093
,bi05
T11908
Ppb
507.7
2.886
.5685
ppc
507.0
4.988
.9837
Ce4iS6
PPD
'861.3
8.588
.°738
Llb707
pp0
4C5,5
;.:-ro
J ;.;i.
OpD
517. i
o . i / 8
1.1V5
Pb2205
PPO
500,5
2.617
.523
V.2924
ppo
506.4
3.466
.6845
ppb
503,5
.8884
.1765
C02286
ops
507 . o
o.io9
. 6582
fig27?0
upD
501.9
i./82
77.05. •.
pCB
500.1
6.5oi
: - • ^
t . J I i
Sei960
ppo
50o . 8
i.392
.3734
Zn2062
ppb
505,6
5.802
1.148
ppb
502.2
.^033
.0803
C'2677
PPC
508 , 3
3.862
.7598
M2576
ODD
5u4.2
W , w**4
??03-7
ppD
500,4
i.OOi
,9714
3niS99
ppD
507.9
2,745
.5405
Si2881
PPD
515.4
.983
.3117
ppb
507.3
4.028
.7939
Cu3247
ppo
503,6
i.665
,5307
MOIOIO
ODD
^ l : • i
"~&~~"
SD^oB
COD
3ji . i
4.113
.3057
Sr42i5
ppo
507,5
.7038
.1397
128
-------
Analysis Report Averages fled 11-27-96 05:45:09 PM page 11
Method: TRIAN6L2 Sample Name: ICB/CC8 Operator: DKH
Sun Time: 11/26/96 13:02 .- Filename: 11269s
Mode: CONG Type: 8 Corr, Factor: 1,00000
uaD 10.: Cusi. Saoi, 10,: Cust. ID,; 39568
Eiems r)g32dO A13082 flsl890 3_249e> Ba4934 8e3130
Units ppo ppP ppP ppP poo ppo
Avga . .2169 7.996 .5723 -1.247 ,5474 .3887
SDev .1506 2.251 1,5/9 .594 .3515 • .0994
»RSD 69.45 28,15 424.1 47.o5 3.08 25,57
Elens Ca5i79 Cd226S C34186 Co228o Cr2o77 Cu3247
Unus ppP ppo ppo ppb pp0 ppp
Avge .5529 -.3110 -1,624 ,56o4 .2558 .0822
SDev 1.534 .1741 4.637 ,4926 ,3343 ,1194
IRSO 2S7.9 55,98 285,5 86,'5 136,5 145,5
ijfUvS DpO ppiil pOC ppD ODD ODD
Nvoe -2.381 ,1624 .4296 -.'085 . lOc-i .2035
SOsv ia.5 .049 .0561 4.18<» .05*- . 4
-------
Analysis Report Averages Wed 11-27-96 05:43:09 PM page 12
Method: TRIANG12 Sample Naie: ICB/CC8 Operator: OKU
Run Tine: 11/26/96 13:16 Filename: 112696
Mode: CONC Type: u , Corr, Factor: i.00000
Lab ID,: Cust, Sipl. ID,: Cust, ID.: 39563
Eie»s ftg32SG A13082 fts!890 B_2496 8a4934 Be3130
Units ppo ppb ppo ppo ppb ppb
Avge -.0104 11.01 ,066? -3.595 .0021 .0515
SDev ,38 6.138 1,991 ,31 .0135 ,031
IR30 3649 55,75 2978 8.523 o48,i 60.26
El snis
Unui
Avge
SDev
••;cr,
anjU
tisas
units
ivga
SDev
3 ft & r-
-»RSU
Eiesis
Units
Avge
SOev
*RSO
Eieais
Units
Avge
Ca3179
ppa
-,o387
.737
115.4
Fe2714
DDD
-.5605
:-.2b3
910.5
Na3 jO^
ppp
-17.01
150.5
883.8
19oO-i
p?D
-2,^04
Cd2255
ppo
-.7250
.Oboi
7,735
K 7oo4
ppn
.1514
.04io
22. 75
N12316
PpD
,2410
.4954
205,6
1960-2
ppp
-2,941
Ce4lS6
Ppo
-.8676
,93oo
108
i.i6707
DDD
. 1 G 15
32,46
P_214«
ppo
o,662
3.694
55,45
Pb220i
PPD
-i.143
Co2286
DPD
.0098
.2165
220o
«g2790
poo
,0860
5054
2202-1
ppb
-.4224
3.333
739
Ssl960
ppo
-2.928
Cr2677
OOP
'-.27<58
,5359
MO ~i
ii . . w
nn2576
Dpb
, u / ^ -•
,02s/
36 , 8*
2203-2
ppo
-1.502
1.096
72,94
SniS99
ppb
,655s
Cu3247
PPO
-.552^
,36;8
103,8
iio2020
PDO
-,i92i
55.55
Sb20o8
ppo
.6521
5.296
505.4
Sr4215
PDD
,0107
SDev
o5.32 95.3B 65.SD
ileus Tii5i9 H1906 V.2924 -2n20o2 S12SS,
unus ppo DDD ODD ppo ppo
Avge ,0419 -,v44i .2071 .4781 -30,17
SOev ,1286 1.667 .5373 ,3255 1.905
SRSD 307.4 176.6 259.5 b8.04 6.315
130
-------
Analysis Repori Averages Wea 11-27-96 05:43:09 ?pl page 13
Method: TRIAN6L2 Saimie Name: IC5AB Operator; DKH
Run Time: 11/26/96 13:21 . Filename: 112696
Mode: CONC Type: I Corr, Factor: 1,00000
Lab ID.: Cust. Sapl. 10,; Cust. 10,: 39566
Eleis Ag328Q A13062 AslS90 8_2496 8a4934 fie3130
Units ppo ppo ppb ppb ppd ppc
Avge 550.1 529300. 507,4 545,4 520,4 504.0
SDev. 1,653 2190 3.708 1.539 2.27 3,405
IRSD .3004 .4138 .7308 .2821 ,4363 .6757
Eieins Ca5179 Cfl2265 Ce4iS6 CoZ236 Cr2677 Cu3247
Units ppb ODD ppo ppc DPP ppp
Avge 4o5900. 47S.5 875.0 489,0 494.o 559.8
SDev 5816 5.051 ,8367 2.736 4.169 4.61-
IR5D ,8192 ,o37S .095o .5596 .3*3
Units ppo ppo ppo PPD pob ppb
.Avge Go2ii. *7b,4 595.6 516.9 507.4 514,4
SDev 164.1 i.lBl 5.559 4.517 9.303 5.71-
tRSO 2.642 ,3755 .9355 ,8352 1,333 1,112
Eieras 1960-1 1%0~2 ?b2203 3el960 Snl899 Sr4215
Units ppo ppo PDD ppo ppo ppo
Avge 525,1 512.5 510,6 516,7 500.S 530,5
SDev 17.14 5.54G 4,977 4.455 - 4,596 1.35
SRSD 3.265 ,712 .9748 .8585 . .9178 ,2545
Eiems HS349 T11908 V.2924 Zn2062 Si288i
Units ppb ppb PDD ppo 0po
Avge 505.9 512.5 505.5 441.2 515.3
SDev 1.196 3,959 2.246 5.9o2 2.018
IRSO ,23o5 .7725 ,4444 1,551 .3951
131
-------
Analysis Report Averages Ked 11-27-96 05:43:09 PM page 14
Hethoa: iR!ANGL2 Saipie Mm: 39568 H8 Operator:
Run Time; 11/26/96 14:06 Filename: 112696
floae: CONC Type: 3 Corr. Factor: 1.00000
Lao ID.: Cust. Supl. ID.: Cust, ID.: 39568
tiens
Units
Avge
SOev
?;RSO
Asi890
ppD
L-2.371
.8126
34.28
8e3130
ppb
L.062S
.0185
29.55
Ca2265
ppb
L-.7324
.0103
1.405
Co2286
ppb
L-.2787
.3368
120.9
Cr2677
ppb
L-.0247
.3668
1483
Mn2576
ppb
L.4889
.0434
3.879
Eieus Ni2316 Pb2203 Sb2068 Sei960
units ppb ppb ppo ppb
Avge L-i.263 L-.4024 L2.018 L-3.060
SDsv .ma .9385 .8511 2.723
IRSt 24.29 233.2 44.16 89
132
-------
Analysis Report Averages rteo 11-27-96 05:43:09 PM page 15
Hetnod: TRIANGL2 Sample Name: 39568 LCS Operator: DKH
Sun Tine: 11/26/96 14:11 -• filenane: 11269b
node: CONC Type; S Corr, Factor: 1,00000
lac ID,: Cust, Smpi. ID.: Cust. ID.: 39568
Eieus Asl890 Be3i30 Cd2265 Co2286 Cr2o77 Hn2576
units ppb ppD ppo ppo ppo ppo
Hvga 44.59 *6.55 46.70 47.30 47.89 48.29
ii-ev 2.154 .3407 ,3799 .7454 .744 ,2466
IR3D 4.831 ,7319 .8134 i.576 1.553 .5107
tiess N12316 Pb2203 5b2063 Sei960
Units ppo ppo ppo pob
Avge 4b,v5 i6,9c' 48.77 43.95
Suev .7799 i.426 1.67S i.132
'»X5D 1.661 3,035 3.4^
133
-------
Analysis Report Averages Wed 11-27-96 05:43:09 PN page ID
Hethoa: TRIANGL2 Sample Name: 146-4-2ftSCD Operator: DKH
Ryn Tiie: 11/26/96 14:17 Filename: 112696
Mode: CONC Type: 3 Corr. Factor: 1.00000
Lao 10,: Gust, Snpi. 10.: Cust. ID,: 39568
El ens Asl890 8e3130 Cd2265 Co'2286 Cr2677 Mn2S76
Units ppb ppb POP ppo ppo ppc
flvge 41,05 150,5 17,9? 22"*. 2 211,5 246.5
SDev 1.993 1.008 ,4404 i.788 1.339 .9338
IRSO 4.355 .o696 2,45i ,78 .6329 ,3789
Eiems Ni23i6 ?b2203 Sb2068 Sei960
Units ODD pDD ppo POD
Avge 433.9 387,1 100,5 1266.
SDev i,582 . 3.163 5,8 9,697
SRSD ,4548 .3171 3.788 .7659
134
-------
Analysis Report
Averages
11-27-96 05:45:09 PM page 17
Method: TRIANGL2 Saipie Nate: 146-4-2ABGD PCS Operator: OKH
Run Time; 11/26/96 14:22 . filenaie: 112696
Mode: CONC Type: S Corr. Factor: 1.00000
Lao 10,; Gust. Sipi. ID.: Gust. ID.: 59568
El ems
Units
ftvge
SDev
WSD
ftsl890
ppb
72,13
2.69
3,729
8eS130
ppb
177.6
1.165
.6561
M2265
ppb
46.17
.6241
1.552
Co2286
PPG
257,8
2.191
.8498
Cr2677
ppo
242.8
1,232
,5073
Nn2576
PPO
275.9
i.lfei
1 f.f, r-
,4iU3
tiems
Units
Avge
SDev
IHSO
H12316 Pb2203 5b20o3 Sel960
ppb ppb ppo pob
460.1 409.9 129.5 12&7.
2,142 5.735 2.313 7,102
.4655 1.S99 l,T5^ .5605
135
-------
Analysis ngport Averages Sued 11-27-96 05:43:09 PM page 18
netnoa: IRIANGL2 Sample Name: 146-4-2A8CO L Operator: DKH
Run Time: il/26/96 14:27 Filename: 112696
floae: CONC Type: S Corr, factor: i.00000
Lao ID.: Gust. Supi. ID.: Cust. 10.: 39568
£le»s fls!890 8e3130 Cd2265 Co2286 Cr2677 Nn2576
units ppb ppb ppb ppb ppb ppo
Avge 13.35 46,60 5,459 69.73 74,oO 69,52
SOev 2.436 ,2434 .1931 .7926 ,6845 .2582
SRSD 17.58 .5224 3.556 1.137 .9175 .3714
ileus >ii2316 Pb2203 Sb206S Sel960
Units ppb ppo ppb ppb
Avge 132.4 122,5 30,61 410,3
SDev 1,38 1.26 1.286 2.446
4RSD 1.042 1.029 4,202 ,5962
136
-------
Analysis Report Averages
*ed 11-27-96 05:43:09 PM page 19
Method: IRIANGL2 Sample Name: 146-4-3ABCOE Operator: DKH
Run Tims: 11/26/96 14:32 Fiienaie: 112696
node: CONC Type: S Corr, Factor: 1.00000
lap ID,: Cust, Srnpi. 10,: Oust. ID.:,39568
Eieiis
Units
Avge
SDev
°;RSD ,
flsl890
ppo
42. 75
4,804
11.24
8e3130
ppo
159.9
1 . 06b
") i • n
, (010
Cd2265
PPD
55.34
,9235
1.669
Co2286
PPO
233 . 0
2.748
1.179
Cr2677
ppo
306.0
2.161
.7061
Mn2576
ppo
1130,
3.53
.3125
ileus
Units
Avge
SDev
IR3D
,Ni2316
ppb
486.6
3.107
.6586
PB2203
ppb
896.?
3.021
.8^46
Sb2068
ppb
98.22
i.Sii
3.57-
3el960
ppb
600.0
3.793
,6321
137
-------
Analysis Report Averages Wed 11-27-96 05:43:09 PM page 20
rtethod; TRIANGL2 Sample Name: 146-4-3A8CDE DA Operator: OKH
Run Tine: 11/26/96 14:37 Filename: 112696
Noae: CONC Type: S Corr. Factor: 1,00000
tab ID.: Cust. Smpl. ID.: Cust. ID.: 39568
Eleas
Units
Avge
SDev
IRSD
Eieais
units
ftvge
SOev
«RSD
Asi890
ppb
42.76
1.811
4.236
N12316
PPD
489.8
i.704
.3479
185130
ppc
141.1
,8811
.6243
Pb2203
ppo
90o,7
3.225
.9072
Ca2265
PPD
55.38
.5629
1.007
3D2068
ODD
101.3
3.543
3. "95
C02286
PPP
236.6
1.194
.504b
381960
ppo
603.2
1.24?
,206o
Cr2677
ppP
308,5
1,5
.4864
ftn2576
PPD
1137,
3.213
.2827
133
-------
Analysis Report, Averages Wea 11-27-96 05:43:09 PM page 21
Method: TRIANGL2 Sample Naie: 146-4-4A8CO Operator: DKH
Sun Tiie: 11/26/96 14:42 • -Filgnaie: 112696
Mode: CONC Type: S Corr. Factor: 1.00000
Lab ID,: Gust. Snpi. ID.: Cust. ID,: 39568
ileus
units
Avge
SOev
IRSD
AS1890
.ppb
32,43
2.811
8.66?
Be3130
ppo
128,6
.663
.5156
Cd226S
PPD
51,64
,1815
.3514
Co2286
PPD
190. S
2.042
i.07
Cr2677
ppo
260,0
i.318
,5068
Nn2576
ppb
955.7
4.015
.4201
Eiems Hi23i6 ?b2203 552068 Sei9&0
units ppo ppo ppD PPD
nvgg 417,7 317,7 91.08 605,S
SDev .9965 5,513 i.773 4.705
ISSO ,2385 ,6745 1,934 ,7766
139
-------
Anaivsis fiepon, Averages Wed 11-27-96 05:43:09 PM oaae 22
Mettioa: TRIAN6L2 Sampis Name: 146-4-5AICO Operator: OKH
Run Tine: 11/26/96 14:47 Filename: 112696
Hoae: CONC Type: S Corr, factor: 1.00000
Lab ID,: Cost. Snoi. ID.: Cust. ID.: 39568
clets
Units
Avoe
SDav
SRSO
AS1S9G
ppb
27.08
2,314
8.546
Be3130
ppb
137.2
,3971
,2895
Cd226S
ppb
11.15
.4835
4.337
Co2286
PPb
203.6
1.55
.7616
Cr2677
ppb
158.1
.7989
.5052
Mn2576
ppb
431.7
1.066
.247
Eleois NJ2316 Pb2203 Sb2068 Sel960
Units ppb ppo ppb ppb
Avge • 385.4 252.1 64.50 420.1
SDev .7804 ,3243 5.199 3,055
%RSD .2025 ,1286 3.06 ,7272
140
-------
Analysis Report Averages rtea 11-27-96 05:43:09 ?H page 23
Method: TRIAN612 Sample Name: H6-4-6ft8CD Operator: DKH
Run Time: 11/26/96 14:52 Filenaae: 112696
Mode: CONC Type: 3 Corr. Factor; 1.00000
Lao ID,: Cust. Sid. 10.: Cust. ID,: 39568
Eiess fts!890 8e3130 Cd2265 Co2286 Cr2677 Mn2576
Units .ppb ppp ppo ppo ppo ppp
fivge 19.55 148.3 10.97 201.9 132.5 403.5
SDev 2.586 ,4671 .409 .8858 2,559 .9037
IRSO 12.2 .315 3,728 ,4386 1.931 .224
Eleiiis ?H25io PD2203 Sb206S Sei960
Units poo ppo pps ppb
fivge 357.3 258,3 59.08 479.3
SDev 2.663 1.31 3.551 2.85
ISSD .8014 ,5075 6,01 ,59
-------
Analysis Report Averages Wed 11-27-96 05:43:09 PCI page 24
rtechoo: TRIANG12 Saupie Haine: ICV/CCV Operator: OKH
Run Time: 11/26/96 15:11 Filenaie: 112696
ftoae: CONC Type: Q Corr, Factor: i,00000
Lab ID.: Cust. Smpl. ID,: Oust. ID.: 39568
ileus
Units
Avge
SOev
IfiSO
Eiaffls
units
Avge
SOev
M5D
Elsfls
U n i t s
livge
SOev
SRSi
Eiens
Units
Avge
SCsv
IRSD
Eieas
Units
AVGc
SOav
IR30
Eiesis
Uni:s
Avgs
SDev
WSD
Ag3280
PPC
511,1
,2568
.0502
Ca5i79
ppo
49",?
2.m
,5406
Fe2"l»
PPB
50o,5
4.918
. .971
Na53C2
ppb
4648,
147
3.163
1960-1
PP«
500,5
1.562
.3121
11334°!
PDD
484,5
i.609
•* -"i A
,«)j<:i
A 13082
ppo
6556,3
1,493
,2o75
Cd2265
PPO
505.2
3.301
,65ol
,<_7oo4
PDPI
; v:o
^ . j ~> •
.0502
,59oi
Ni231o
pps
507.2
6.539
1,289
1960-2
ppb
510.1
5.01
.9823
TI1903
PpD
498,4
5.404
1 A(", i
I,uo4
AsiS90
Dpb
508.5
i "\ 7 1
i.tQl
.4399
Ce4i86
ppD
849,3
4,s42
,5465
Lio707
POD
4o3.a
4.45
.955a
?_2i49
PPD
520.?
4.553
.874
PD2203
ppb
4^5,3
3,iA9
.&9b
-------
Analysis Report Averages dea 11-27-96 05:43:09 PH page 25
Method: TRIANGL2 Sample Nane; ICB/CCB . Operator: OKH
Run Tine: ii/26/96 15:17 Filename: 112696
rioae: COHC Type: Q Corr. Factor: 1,00000
Lab ID.: Oust. Snpl. ID.: Cust. ID.: 39568
Elems Ag328Q ft!30B2 Asl890 B_2496 8a4934 Be3130
Units ppb ppb ppo ppb ppb ppo
Avge -.1087 085.29 -.7794 407,7 .5328 .6592
SOev .3266 3.964 2,961 66.64 .0565 .1056
1RSD 300,3 4.647 582.5 16,35 16.98 16,02
Eieits Ca3i"9 Cd2265 Ce4186 Co2286 Cr2677 Cu5247
Units ppp ppb ppb PPD ppp ppo
Hvge -i.loi -.3746 -.9798 ,30/4 ,26*0 -.945':
SDev ,837s ,0411 4,755 ,1239 ,2/46 .251
«RSD 20.13 10.9o 485.5 *0,25 9o,i7 2i,-4
iia^.^if
ODD SOD
.-06-2 -5
iUSV
SFS'D
Eless
liniis
Avge
SOev
IRSO
Eiems
Unics
Avge
SOev
IR30
tleis
Units
flvga '
SDsv
5RSO
-,
N*
V' Z
5. 1
5) 02
P?b
-
72
^7
19
155,0
,°1
.04
oQ-i
ppb
•1
5.
19
"7 "I i
4?
7.4
,v4o
21.7
£j i .' ^
OpD
.* A
5
IF,
55
.;Jc-
24.
a ~_
PPO
6,
,40B2 5.2
50.o
1960
POD
-5.
5.78
167
1
-2
464
3
7i534<5 1 11908
ppo
fv
. lr
25
5855
897
75
ppD
j2.
?b2
ppb
*i
1,0
68.
V_2
ppp
-.5458 i.
2. "8
455.
1
•j
.42
50.
C"3
^, /
i-9
207
38
1 7
203
.525
43
37
=24
331
36
00
o.ib
752.3
2205-i
ppp
-.0741
,6303
851.1
8ei9cO
Ppb
-1.388
4. So;
329.1
Zn2062
PDD
'.5551*
.5303
95.59
, w /'
21.
2iO
PPD
~ /
1.6
1 4 ,
V •
-"•
5"2
,24?
85
91
Snl899
PPD
,4
.50
114
si;
ppb
388
33
•7
881
.46J;
39c-
5020o
ppo
.757
i , i i 0
164.3
Sri/1
PPD
,325
,0b97
21 .55
5
3
5
8
2554.
fO.
5,5
32
So
143
-------
Analysis Report Averages «ed 11-27-96 05:43:09 PM page 26
flethoa: TRIANGL2 Sample Name: 146-4-SA8CDE Operator: DKH
Run Tiie: 11/26/96 15:24 Filename: 112696
Woae: CONC Type: S Corr, Factor: 1,00000
lab ID.: Cust. Smpl. ID.: Cust. ID.: 39568
Elems
Units
Avge
SDev
IRSD
fts!890
ppb
25.41
1.475
5,805
8e3130
ppb
L-.6512
.1091
16.75
CC2265
ppo
L-1S.04
.329
2.188
Co2286
ppb
L-35.20
.9922
2.819
Cr2677
ppb
198.1
1.272
.6419
Mn2576
ppb
242.5
1.579
.6512
Elenis
Units
Avge
SOev
«SD
Ni23l6 Pb2203 Sb2068 Sel960
ppb ppb ppo ppb
136.2 33,71 101.0 96.71
1.325 2.075 2.o6l 1.394
.9726 6.156 2.635 1.442
144
-------
Analysis Report Averages Wea 11-27-96 05:43:09 PM page 27
Method: TRIAN6L2 Sample Name: 146-4-9A8CDE Operator: DKH
Run Tiie: 11/26/96 15:29 Filename: 112696
Mode: CONC Type: S Corr, Factor: 1.00000
Lab ID.: ' Gust. Sipl. ID.: Cyst. ID.: 39568
Eiens
Jnits
Avge
SDev
SRSD
AS1890
ppo
14.50
2.026
13.97
8e5130
ppp
L-17.32
.1359
.7845
Cd2265
ppo
L-.9109
.2682
29.45
Co2286
ppC
10.29
.9325
9.059
Cr2677
PPP
171.7
2.356
1.372
Mn2576
PPP
150,9
.4873
.323
Elenis Ni2316 Pb2203 3b2068 Sel960
Units ppb ppb ppb ppb
flvge 59,75 51.74 26,38 23.42
SDev 1.463 1,52 5,374 .8*42
ifiSu 2.449 2.938 19.99 3.60S
145
-------
Analysis Rsoort Averagss Xea 11-27-96 05:43:09 PM pagi 2B
Method: TRIAN6L2 Saaple Name: 146-4-lOAiCDE Operator; OKH
Run Time; 11/26/96 15:34 Filename: 112696
Mode: CONC Type: S Corr. Factor: 1.00000
Lao ID,; Cust. S»pl. 10,: Cost. 10.: 39568
El8*S
Units
iivge
SDev
SRSD
AS1890
ppD
6.995
2,331
33,32
ie3130
ppD
L.2222
,0574
25,85
Cd2265
ppb
L-4,313
.3594
6,333
Co2286
ppD
L-18.35
1,422
".754
Cr2677
ppc
100.9
2.15
2,131
Mn2576
PPD
99,69
.4421
.4434
Eleis N12316 Pb2203 3C2068 Ssl960
Units ppo pps ppb ppb
Avge 103.9 45.85 43.54 ' 42.65
SDev .3824 4.134 2.947 3.243
-»RSD .3682 9.015 6.769 7.o02
146
-------
Analysis Report Averages ded 11-27-96 05:43:09 PM page 35
Method: TRIAN6L2 Saipie Naine: ICV/CCV Operator: DKH
Run Time: 11/26/96 16:10 Filename: 112696
node: CONG ' Type: 9 Corr. Factor: 1,00000
Lao ID,: Cust. Smoi, ID.: Cust. 10.: 39568
Eieas
Units
.Avge
Suev
ifiSD
tlens
Units
Avge
SOev
%sso
•iSK
Uniis
Avge
SOev
*.RSO
ciejis
Units
Avgs
5Dev
-MSO
Elans
uniis
Avge
SOev
iRSD
-Eiens
Units
Avge
SOev
IRSO
$03280
opo
515.5
1,426
.2766
Ca5179
ppO
0598,?
34.48
5,753
Fa27l4
ppo
517,2
M96
1.391
Nao502
ppo
«44o4.
21i.7
4. Si
1960-i
ppo
498,0
* . 963
.99oo
"i5o49
ppb
48V, /
1.281
,2616
A13082
COP
Q611.0
7.694
1.259
Cd2Z65
ppb
514,5
2,277
,442ft
KJ664
ppra
4.941
.043
,8699
Ni25io
PPD
518,2
2.213
,427
1960-2
DOO
515.7
4.315
,9373
111908
ppb
50i,5
7.512
1.492
AS1890
ppo
514.7
2.256
,4383
Ce4186
ppb
850.4
1 ,6d4
.1957
Li6707
SpO
Q442,o
/' . 030
1,729
?_2id9
ppD
528,5
4,872
0" t ~
Pb22C3
ppo
504,9
1.461
, 2894
V_2924
ppb
505.5
,3367
,0666
B.2496
POD
•513.
243.1
16.07
Co2286
ppD
504,1
1.553
.308
iig2790
OOP
500.9
,?304
2203-i
ppo
479,0
3.551'
,7412
Sei9oO
ppb
508.4
i.559
, iC'66
in2062
ppo
5i9,0
4,676
,901
Sa4954
ppc
499,7
,;759
,0352
Cr2677
pnb
516,3
1.931
.57a
.1n2576
ppo
502,0
1.3*;
,366*
2203-2
pob
517. S
3.8o7
."4oo
3ni899
ppo
496,7
3.695
.7438
512881
ppb
29360.
4303
14.66
8e3150
ppb
508,4
3.091
.6079
Cu3247
ppb
497.4
1,522
,30o
R02020
DPD
512.5
5. GO"5
-58/4
Sb2C68
ppD
522,3
1,28
.2448
Sr4215
ppO
493.6
.4712
.0945
147
-------
Analysis Report Averages Wed 11-27-96 05:43:09 PC! page 36
Method: IRIAN6L2 Sample Name: IC8/CCI Operator: DKH
Sun Time: 11/26/96 16:16 Filename: 112696
node: CONC Type: 0 Corr, Factor: 1.00000
Lab ID.: Gust. Smpl. ID.: Gust, ID.: 39568
Eiens
units
Avge
SOev,
IftSD
Eiens
units
Avge
SOev
•sRSD
tieras
units
HVC8
SDev
:;RSO
Eieas
Unus
Avge
SOev
iRSD
liens
Units
4vge
SOev
4RS&
Eieras
jnit;
Avgs
SOev
IRSD
Ag3280
ppb
.5114
.3133
100.3
Ca3i79
ppo
5.202
i , / /
53.26
re27i4
PPD
4.1*2
3 . 335
Io5
.133302
PPD
.-117. 2
51,23
2o.65
1960-1
ppb
-1,498
2,876
It] ,~i
71334?
ODD
.3998
.2045
. 34.1
A130S2
ppb
3123.5
8.023
6.495
Cd'2265
ppb
-.3486
.1409
40.4
&_7664
pom
".2577 '
.0342
a, 47
Hi231b
ppD
1.259
.7692
6i.09
1960-2
ppb
-2.501
.7455
32.4
T11908
ppo
.1137
4.391
~> 0 " "t
joou
AS1890
ppD
1.205
.4469
37.08
Ce4io6
ppb
,0126
1.917
15220
Lio707
PPD
,5014
.0911
15.16
P.2149
PPb
5.445
7.96
146,2
Pb2203
ppb
-.2726
2.092
767.6
V.2924
PPD
Q2.576
,2274
8.827
8J496
Ppo
1040,
179.4
17.25
C02286
PPD
.4580
.2582
5o.36
,1g279'0
ppD
4,55i
1.363
-2,5
2203-1
ppO
2.129
o.59i
309.5
Sel960
ppb
-2,03i
.4609
22.66
in20o2
ppb
.525o
.2927
55.69
Ba4934
ppb
,4367
.1803
41.3
Cr2677
ppo
1.617
.5919
24.23
Mn2576
opfi
.51^5
,1367
26.56
2203-2
ppb
-i.472
1.762
119.7
3nl8q9
ppD
1.064
.5573
52.38
Si2881
ppo
12700.
881.?
6.944
6e3130
ppb
.9680
.2109
21.79
Cu3247
ppb
-1.885
,3986
21.16
no2020
PPD
-i!S2
,4236
194,5
Sb2068
PPD
1.355
2.058
112.2
Sr4215
ppb
.4557
.1548
35.97
148
-------
Analysis Report Averages idea 11-27-96 05:43:09 PH page 57
Method: TRIANGL2 Saiple Naie: 146-4-11A8CDE Operator: DKH
Run Time: 11/26/96 16:29 Filename: 112696
floae: CONC Type: S Corr, Factor: 1.00000
Lab ID,; Oust. Sipl. ID,: Cust. ID,: 39S&8
Eleis
Units
Avge
SDev
IRSO
Asl890
ppb
L2.239
1.459
65,16
Be3130
ppt)
L.4950
.0476
9.614
M2265
ppb
L-2.228
.2086
9.361
Co2286
ppo
L-9.091
.3015
3.317
Cr267?
ppb
63.12
.7386
1.17
Hn2576
PPB
49.52
,2479
.5006
Eleis
Units
Avge
SDev
»<;sn
*Ji* UM
N1231&
pp6
32.64
.4453
i ,364
?b2203
ppo
13.75
.3688
0.327
Sb2068
ppb
27.89
.7689
2,157
Sel96fl
poc
21.42
1.802
6.411
149
-------
Analysis Report Averages Wea ii-27-96 05;4i:09 PH page 38
Method: TRIftNGLZ Sample Name: 146-4-12ABCE Operator: OKH
Run Time: 11/26/96 io:34 Fiisname: 112696
iloce: CONC Type: S Core, Factor: 1.00000
Lao 10,: Gust. Snpl. 10.: Cust. ID.: 39568
tlens
Units
Avge
SOev
«so
Asl890
ppb
12.35
1.837
14.87
8e3130
ppb
L.5724
.0239
4.179
Cd2265
ppb
L-12,03
.1807
1.501
Co2286
ppn
1-25.16
.7472
2.97
Cr2677
ppt)
147.0
i.65
1.123
Hn2576
ppb
13.77
.2105
1.528
Elans
Units
Avge
SOev
IRSO
Ni2316
ppo
86.95
.9504
1.07
Pb2203
ppfa
22.42
1 .945
8.672
Sb2068
ppb
73,54
4.278
5,317
Sel960
ppb
68.22
2. 988
4.38
150
-------
Analysis Reporc Averages
«ed il-27-96 05:43:09 PM page 39
Method: TRIANG12 Sample Name: 146-4-12D
Run Tine: 11/26/96 16:39 Filename: 112696
Corr, Factor:
Mode: CONC
lab 10.:
Type: S
Cust, Sipl. ID.
Gust.
Operator: OKH
1.00000
10,: 39568
Eiens
Units
Avge
SOev
IRSD
AS1890
ppb
L-4.916
1,433
2
-------
Analysis Report Averages Wed 11-27-96 05:43:09 PM page 43
Method: TRJftNGi.2 Sample Name: 146-4-2flBCO Operator: OKU
Run Tine: 11/26/96 17:09 Filename: 112696
Mode: CONG Type: S Corr. Factor: 1,00000
tab 10.: Cust, Snoi. ID.: Cust. ID.: 39563
Eieis
units
Avge
SDev
*.RSO
Eiens
Units
Avge
SDev
IRSD
fts!890
ppD
43.95
0 CSG
i, . JQ>
5.89
Ni231i5
ppo
449.0
.2851
.0635
ieJlSO
ppb
149. 1
\M1
.673
P0220S
ppb
416.9
3.457
.3293
Cd2265
ppo
16.67
.4983
2.989
Sb2068
ppb
108,7
3.213
2.955
Co2286
ppb
242.6
2.751
1.134
Sel960
ppb
1289.
12.4
.9624
Cr2677
ppo
215.9
i.118
.5177
Hn25/6
ppb
249,6
1.072
.4292
15
-------
Analysis Report Averages Wea 11-27-96 05:43:09 PM page 44
Methoa: TRIANGL2 Sample Naie: 146-4-2ABCD POS Operator: DKH
Run Tide: 11/26/96 17:14 Filenane: 112696
Mode: CONC Type: S Corr, factor: 1.00000
Lab ID,: Cust. Sipl. ID,: Cost, ID,: 39568
Elerns Asl890 6e3l30 Cd226S Co2286 Cr2677 Nn2576
Units ppb ppo ppb ppb ppc ppb
Avge 194.2 293.1 170.1 392.8 377,8 407,3
SDev 2.909 1.85 1,433 2.56 2.2 1,678
SRSD 1,495 .6315 .8423 ,6516 .5623 ,4119
Eiems Hi231b Pb2203 Sb2063 Sei960
Units PPD ODD ppo opo
ftvge 585.5 551.5 261.5 1382.
SOsv i.375 4,259 3,208 - 8,64c
-"•?-,- T -j ft T i n *". "1 •• ,~. r ~
, oiOo ,//io i.tt/ ,Oi3S
153
-------
Analysis Report Averages ded 11-27-96 05:43:09 PM page 45
Method: TRIANGL2 Saupie Name: 2-110-4 SQOuL/lOnis Operator: OKH
Run Tine: 11/26/96 17:25 Filenate: 112696
node: CONC Type: S Corr. Factor: 1.00000
LaD ID,: Cust, Sipi, 10.: Cust. ID.: 39568
Elens
Units
Avge
SDev
«SD
tiens
Units
Avge
SOev
4RSO
AS1890
ppb
281.1
1.143
.4055
Hi23i6
ppb
273. 2
2.72?
.980^
BeilJO
ppo
272.3
2.122
.1793
Pb2203
ppb
270.2
2.363
.8761
Cd2265
PPC
275.9
2.12
.7682
Sb2063
ppb
283.0
4,165
i.472
Co2286
ppb
272.0
2.1
.7722
3el960
ppb
279.6
.647
.2314
Cr2677
ppb
276.4
2.058
.7445
Mn257e
ppb
271.9
2.212
.8157
154
-------
Analysis Repori Averages Hed 11-27-96 05:43:09 PM page 46
iletnoa: IRIANSL2 Sample flame: ICV/CCV Operator: OKH
Run Tiie; ll/2o/96 17:30 ' Filename: 112696
iloae: CONC Type: Q Cor--, factor; 1,00000
Lao IB.: Cust, Smoi, ID.: Cust, ID.: 39568
Eleois Ag3280 A13082 Asi890 8_2496 8a4934 8e5130
Units ppb ppp ppo ppb ppo ppo
Avge 510.9 3612.0 516,5 1607. 497.0 505.3
SDsv .3501 4.985 1,315 33.1 .6292 2.171
IRSD .0685 .8145 ,2545 5.482 .1266 ,4297
ElsiiS Ca3179 Cd22o5 C84136 Co2286 Cr2677 Cu3247
Units ppD ppp ppb ppp poo ppo
Avge 516.2 509,9 342,3 500,0 508.6 494.5
SDev 5.104 1,575 3,?~s 2,145 2.31 .6352
SRSD ,601i .3CS5 .4721 ,429 ,i659 .1686
i1g2790 Hn257o ilo2G2C
pp6 ODD DDD
503,7 493,3 507,7
3.593 i.oi9 1.155
:ia3302 ;ii23l6 :_21-9 2203-i 2205-2 SD20o3
DOC ppo ppD ODD ppD DDD
0*402, 51*.3 528,* »77.9 508.0 516.3
115.4 ,o51 3,52d i.362 4.384 3,175
2.577 ,1227 1,614 .8082 .8629 I.G02
Elefjs
Units
Avge
SDev
IRSD
Elans
Units
Avge
Suev
IRSD
1960-1
PPD
500.8
1.981
.5955
T13349
ppb
484.2
1.418
.293
1960-2
DDD
509,4
3.009
.5906
711908
ppP
500.0
3.45o
.6912
PP2203
ppb
493.0
1.81s
,3647
V.2924
ppp
500,4
1.58
.3158
Sel960
ppD
506.6
2,62o
.5184
Zn2062
pop
515.0
3.563
.6531
Snl899
ppo
49o.8
2.062
.415
Si288i
PPP
5758.
252.1
4.379
5r4215
DDP
495.4
.684
.1381
155
-------
Analysis Report
Averaaes
11-27-96 05:43:09 PM page 47
Method: TRIAN6L2 Saiple Nane: IC8/CC8 Operator: OKH
Run Tine: 11/26/96 17:35 filename: 112696
node: CONC Type: Q Corr. Factor: 1.00000
ub 10.: Cust. Smpl. ID.: Cusi. 10,: 39568
Ag32SO A130B2 Ssl690
ppo ppo ppD
99.07 5.883
le4ii)6
ppD ppb
-.2760 .1199
,1801 1.655
65.24 I3e3
tisms
Units
Avge
SDev
IRSO
S_76s4 Lio707
OBIil ppC
46.29 /'3.939
111908 VJ924
ppb pp&
82.5ci
1.606 .4244
Si283i
ppb
4446,
Zn2062
ppo
i',160
.4325
156
-------
Analysis Report Averages Wed 11-27-96 05:43:09 PM page 48
ilethoo: TftIflNGL2 Saapie Name: ICB/CCB Operator; OKH
Run Time: 11/26/96 17:41 Filename: 112696
Mode: CONG Type: Q Core, Factor: 1.00000
Lab ID.: Gust. Srool. ID.: Cust. 10,: 39568
tiens
Units
3vge
SDev
«SO
Eless
•jnics
ivge
SOev
MSO
•Eiests
Unus
Avae
SDev
iRSD
Elsies
Units
ftvge
SDev
?,RSD
Eieras
Units
Avgs
SDev
tfiSD
Elens
uniis
ftvge
SOev
IRSO
Ag5280
ppfi
-.0241
.380?
1579
Ca3179
ppo
-4,734
,Q65"
20.4
Fs27l4
DpD
-1.421
6.532
459.3
Na3302
DpD
-06, 15
00,^2
95,58
1960-1
ppb
1.065
3.349
514,9
7133*9
Opb
.1566
.1081
69.01
A13082
ppb
8124.4
7.065
5,o8i
W2265
ppo
-.7107
\ ? T S
;7.58
KJ664
ppn
,506o
,0388
12.66
N12316
ppo
.5390
.7552
140.1
1960-2
PPD
-1.396
2.935
210.1
T11908
pp0
-4,106
1.199
29,21
AS1890
ppb
.6117
2.512
410.7
Ce4l6o
ppb
- tOGO
. '1 u / ^
n "> 7T
538,6
Lio707
ppo
._ j.-
.055o
23.95
P_2l49
ppo
/ ,o6y
,?4i8
9.429
Pb2205
ppb
1,026
1.57
153.1
V.2924
ppb
32.209
.4337
19.64
B_2496
PPD
912.3
106.5
11,68
Co228o
ppo
.3^35
.296
86. 16-
Mm
PPD
0 . (JLL
0 , ^ j i.
210,2
2203-1
-PPD
i . o 1 4
1.682
50.75
Sei960
ppb
- c 1 7 1
3.062
550.3
In20o2
ppo
,4333
.1622
37,44
8a4934
ppc
.0^30
'to1??
> V L i. -
24.16
Cr26//
ppo
,3319
,4672
139.5
In257=
P&D
. 10-i
,054^
35, 3^
?'"fl"-"
PPD
-.Iio6
2.182
1871
Snl8o:
Ppb
.0536
1.25
3715
Hid'Oi
ppo
400o,
39. ii
2,224
8e5130
ppb
.o388
,0601
9.407
Cu3247
PPD
3-2.085
.25o8
! 0 ? "
i i . '-. i
H02020
PPD
-.ooii
.3135
3£ , QO
3b2068
ppo
.5*21
1,429
263,6
Sr42i5
ppb
,0916
.0214
23,58
157
-------
i/sii ;.ecor: Average; ^ed ii-27-% 35:43:09 PM page 49
iietnod; TRIANSL2 Sample Name: ICSAS Operator: OKU
Run lime: 11/26/96 18:01 fiienaie: 1126%
noae: CQNC Type: Q Corr. Factor: 1.00000
Lao ID,: Gust. Sapl. ID,: Cust. 10.; 39568
ileus Ag3280 A13082 AslS'O 8_2496 Ba4934 3eS130
Units ppo ppD ppc ppb ppD opo
ftvge 562.4 535100. 519,2 1570, 531.4 503.1
SOev .3347 1929 1.18 128. i 1.623 2.295
5RSO ,1484 .3605 .2272 •• 8.159 .3065 .4562
Ca5i"9 Cd2265 CeilS6 Co2286 Cr2677 Cu5247
DpO pp& ppo ODD ppD pDP
467400. 487.3 370.5 490.5 501,5 567.5
2381 1.773 3.0D9 i.879 2.747
,5v?i ,3o35 .44J5 ,3331 .5475
1:6/0'' >!Ci790 '•'n/S/c No.020
DPC ppo ODD ODD
Ovb.i ;j3iOO. 541,7 -So.;-
2,9o3 li:8 1,024 .3221
.4QO& ,2086 ,3736 .16*°
Eisss H«33C2 Hi2316 P_2;49 2203-1 2203-2 SbZOtS
Units DOD ppD ppo poo PDD poo
Avce ;oto. 488,3 573.0 504,7 519.5 525.o
SDsv 92.3o .451 12.42 6.448 5,162 5.n6
IfiSD i.o3 ,0923 2,163 1,277 ,993b ,7451
tieis 1960-i 1960-2 Pb2203 Sel960 3nl899 Sr42i5
Units poo ppP ppc poo ppb ppc
Avge 528.7 527,3 514.6 527.8 490.0 552.3
SOev ii.21 5,117 1.577 1,609 2,171 1,1-4
%RSD 2,o88 .9705 .2676 ,30*9 .443 ,2243
Eleffls 713349 T11908 ¥_2924 Zn2062 3125S1
units ppo ppo poo ppa ppb
Avge 497,3 507,9 507.2 -449.2 5820.
SDsv 1.544 18.09 4,577 2.754 124.8
iRSO ,2701 3.5o2 .362? .613
-------
HUT; o s«rap j. ei" i_u«u i uy i«i
-------
' BE-SEL
Print Data: Main+Suppl,
Print: Calib. Curve
Analyst: HOLBTE
Peak Storage; 1 Repl./Sample
INSTRUMENT: 4100 ZL
Wavelength: 234.9 Peak
Signal Type: Zeeman OA
Read Time: 3.0
Sample Replicates: £
Standard Replicates: £
Techniques HGA Versions 7.3®
Slit: 0.7 Low
Signal Measurements Peak Area
Read Delays 0.0 BOC Times 2
Spike Replicates: Same as Sample
CALIBRATIONS
Sol ut ions
Calib. Blank
Standard 1
Standard £
Standard 3
Reslope Std.
Samples
ID
STD BLANK
STD1= 2ug/L
STD£= 5ug/L
STD3= HZiug/L
5ug/L
Cone
_. «««.*«_
a. 00
5.00
10.80
5. 00
Locat ion
0
1
1
£
1
Vol ume
10
4
10
10
10
10
Diluent 1
Volume 1
5 I
11 1
5 1
5 1
5 i
5 1
Diluent Location: 0
Modifier #1 Location: 48 Modifier #£ Locations
Calibration Units: ug/L Sample Units: ug/L
Calibration Type: Linear
Modifier
#1
5
5
5
5
5
5
#2
Furnace Time/Temperature Program:
Step
1
o
3
4
5
Temp
I 110
130
1 1 500
1 £300
I £500
In j ect i on
Ramp
1
1
5
0
1
Temp
Hold
£5
£0
15
3
5
Gas Flow
250
£50
250
0
Read
*
£50 i
Gas Type 1
Norm 1
Norm I
Norm 1
Norm I
Norm I
: £0 Pipette Speeds 85%
Extraction ..System: On
SEQUENCE:
Step Action and Parameters
1 Pipet diluent + modifier 1
£ Run HGA steps 1 to End
+ spike -t- sample/std
CHECKS:
Recalibrat ion Types
Locations: None
Reslope
Cone. Above Calibration Action; Dilute
Alternate Sample Volumes £0.0 and Concentration > 0. 2
Check 54RSD on: Samples + Standards + Spikes
Recovery Measurements:
5 uL of 5 ug/L Standard at Location 1 Gives
Measure Recovery on Samples: 9—10,16-17
Add to QC Samples: Yes % Recovery
then Retry 1 times
QC Samples
2.50 ug/L
Limits: S5 to 115
160
-------
#i fl/S I QC Sample I Cone. Limits I AfterIPeriodicIftt ICount flsI
! Loc. I ID 1 Lower Upper ICalibl Check I End I Sample I
1 4 ICV=3.0ug/L £. 7 3. 3
2 0 ICB -1.0 1.0
3 5 CCV=6.0ug/L 4.8 7. £ X XX
4 0 CCB -1.0 1.0 X X X
Run Periodic QC Samples; Every 10
Out of Limit fiction* Reslope and Rerun Samples
Matrix Check Calculations:
% Difference for Dupls: No Locations:
"/• Recovery for Spike: No Locations: Cone:
161
-------
Element File: BE.GEL
Date: l£/0£/96
Data File; EB012.DOT
Technique: HGA
Element: Be
Times 14:25
ID/Wt Files EB012.IDW
Calib. Type: Linear
Wavelength: £34. 9
Slit: 0.7 L
Lamp Current: 30
Energy; 69
Be
ID: STD BLANK
Seq. No.: 0000£
A/S Pos.: 8
Dates 12/02/9&
uL dispensed: 5 from 0, 5 from 40, 10 from 0
Replicate i Times 14:£7
Peak Area (A-s): -0.000 Peak Height (ft): 0.003
Background Pk Area (A-s>: 0.003 Background Pk Height (ft): 0.009
Blank Corrected Pk Area (A-s): -0.081
Concentration (ug/L >: -0.05
uL dispensed: 5 from 0, 5 from 40, 10 from 0
Replicate £ (Peak Stored)
Peak Area : 97. 81
Be
ID: STD1= £ug/L
Seq. No.: 00003
A/S Pos. : 1
Date: l£/0£/9fc
uL dispensed: 11 from 0, 5 from 40, 4 from 1
Replicate 1
Peak Area (A-s): 0. 0£0
Background Pk Area (A-s): 0. 037
Blank Corrected Pk Area (A-s): 0.020
Concentration (ug/L ): £.01
Time: 14:32
Peak Height (A): 0.075
Background Pk Height (A)-j 0:125
uL dispensed: 11 from 0, 5 from 40, 4 from 1
Replicate £ (Peak Stored)
Peak Area (A-s): 0.019
Background Pk Area (A-s): 0.038
Blank Corrected Pk Area (A-s): 0.019
Concentration (ug/L ): 1.90
Mean Cone (ug/L ):
1.9&
Standard number 1 applied. C£.003
Correlation coefficient: 1.00000
Time: 14:34
Peak Height (A): 0.087
Background Pk Height (A): 0.147
SD: 0.07&
Slope: 0.0099
RSDC/.) : 3. 91
Be ID: STD£= 5ug/L Seq. No. : 00004
uL dispensed: 5 from 0, 5 from 40, 10 from 1
A/S Pos.: 1
Dates 12/02/9&
Be
ID: STD1= £ug/L
Seq. No.: 00005
A/S Pos. s 1
uL dispensed: 11 from 0, 5 from 40, 4 from 1
Replicate 1 Times 14:4£
Peak Area (A-s): 0.0£0 Peak Height (A)s 0.067
Date; 12/02/96
16
-------
Blank Corrected Pk Area (A-s): 0. 0£1
Concentration (ug/L ): £.08
uL dispensed: 11 from 0, 5 from 40, 4 from 1
Replicate 2 (Peak Stored) Time; 14:44
Peak Area (A-s): 0.0£0 Peak Height (A): 0.093
Background Pk Area
-------
*8i§Blay Calibration -
* -I
a
0.0
Cone entrotlon
fl.»*4«
10.00
164
-------
Element File: BE.GEL
Datei 12/82/96
Data File: EB012.DftT
Technique: HGfl
Element: Be
Time: 14:55
ID/Wt File: EB01S.IDW
Calib. Type: Linear-
Wavelengths £34.9
Slit: 0. 7 L
Lamp Current: 30
Energy: 70
Be
ID: ICY=3.0ug/L
Seq. No.:
ft/S Pas.: 4
Date: 12/02/96
uL dispensed; 5 from 0, 5 from 40, 10 from 4
Replicate 1 Time: 14:57
Peak ftrea (fl-s): 0.027 Peak Height (ft): 0.102
Background Pk ftrea
-------
Peak ftrea (ft-s): 0. ®09
Background Pk Area (ft~s> : 0.0£0
Blank Corrected Pk firea (ft~s>: 0.809
Concentration : 0.000
Concentration (ug/L >: 0.05
uL dispensed; 5 from 0, 5 from 40, 10 from 7
Replicate £ (Peak Stored)
Peak Area (ft-s): 0.000
Background Pk Area : 0.00®
Concentration (ug/L ): 0.03
Time: 15:14
Peak Height (A): 0.00£
Background Pk Height (A)
0.011
Mean Cone (ug/L > :
0. 04
SD: 0. 008
RSDC/.) s 19. 99
Be ID; 39568$ LCS2.X10
Seq. No. : 000 IS
A/S Pos. : S
Date: l£/0£/96
Cf
uL dispensed; 5 from 0, 5 from 40, 10 from 8
Be ID: 395&8$ LCS X10
Seq, No.: 00013
A/S Pos. : 8
Date: 12/02/96
uL dispensed; 5 from 0, 5 from 40, 10 from 8
Replicate 1 Time: 15sl9
Peak Area (A-s): 0.045 Peak Height (ft): 0.201
Background Pk Area (ft-s): 0.0S1 Background Pk Height (A); 0.384
Blank Corrected Pk ftrea (A-s): 0.045
Concentration (ug/L ): 5.08
uL dispensed: 5 from 0, 5 from 40, 10 from 8
Replicate £ (Peak Stored)
Peak Area (A-s): 0.045
Background Pk Area (A-s): 0.080
Blank Corrected Pk ftrea (ft-s): 0.045
Concentration (ug/L )s 5.0£
Time: 15:21
Peak Height (ft): 0.195
Background Pk Height (A): 0.303
Mean Cone (ug/L ) :
5.05
SD: 0.043
RSDC/t) : 0.86
Be
IDs 146-4-lftBC X50
Seq. No.: 00014
ft/S Pos. s 9
Dates l£/0£/9(
uL dispensed: 5 from 0, 5 from 40, 10 from 9
Replicate 1 Time: 15s£4
Peak Area (A-s): 0.035 Peak Height (ft): 0.130
Background Pk ftrea (ft-s)s 0.071 Background Pk Height s 0.£20
Blank Corrected Pk ftrea (ft-s): 0.035
Concentration (ug/L )s 3.94
16G
-------
Replicate £ (Peak Stored) Time: 15:26
§eak ftrea,(QrsXs 0.039 , _ ,__ 6'eak Hei qht.-Xft.). : . 0£ 150_ , _, ^ , _
acRground Pk Area YH-S): 0.075 BacRgroufld Pk Heigftt; ; 3.09
16'
-------
Replicate 2 (Peak Stored) Time: 15:41
Peak Area (ft~s): 0.038 Peak Height (ft): 8.104
Background Pk ftrea
-------
Peak ftrea (A-s): 0.001
Background Pk Area (fl-s): 0.005
Blank Corrected Pk ftrea (ft-s): 0.001
Concentration (ug/L ) ; A fflfl
Peak Height (ft): 0.003
Background Pk Height (ft): 0.024
Mean Cone (ug/L )
0.04
SDs 0.05£
RSDCX) : 122. 15
Be
ID: 39568 LCS
Seq. No.: 00040
Pos. s 1!
Date; 12/02/96
uL dispensed: 5 from 0, 5 from 40, 10 from 15
Replicate 1 Time: 19/:01
Peak flrea (ft-s): -0.000 Peak Height (fl): 0.003
Background Pk Area : 0.005 Backg/ound Pk Height (ft)s 0.019
Blank Corrected Pk flrea (fi-s): 0.000
Concentration (ug/L ): 0.01
uL dispensed: 5 from 0, 5 from 40, 10 frecm 15
Replicate 2 (Peak Stored)
Peak flrea
-------
Blank Corrected Pk Area (fi-s): 0.064
Concentration (ug/L >s 7.17
Mean Cone (ug/L >5 7. 0£ SDi 0.204 RSD<%): £.91
QC sample is within range 4. 8 - 7.2
Be ID: CCB Seq. No.: 00043 A/S Pos. : 0 Date: 12/®£/9fc
uL dispensed: 5 from 0, 5 •from 40, 10 from 0
Replicate 1 Time: 19:16
Peak Area (ft-s): -0.800 Peak Height (ft): 8.00£
Background Pk ftrea (fl-s): 0,005 Background Pk Height (A): 0.022
Blank Corrected Pk ftrea (ft-s): -0.000
Concentration (ug/L )s -0.04
iiL dispensed! 5 from 0, 5 from 40, 10 from 0
Replicate S (Peak Stored) Time: 19:18
Peak flrea
-------
Be ID: CCV=6.0ug/L Seq. No.: 00045
uL dispensed: 5 from 8, 5 from 40, 10 from 5
A/S Pos. : 5
Dates 12/02/96
Be
ID: 39568 MB
Seq. No.: 00046
ft/S Pos.: 14
uL dispensed: S from 0, 5 from 40, 10 from 14
Replicate 1 Time: 19:37
Peak Area : 0.000
Background Pk Area (A-s): 0.005
Blank Corrected Pk Area (fi-s): 0.000
Concentration (ug/L ): 0.05
Time: 19:39
Peak Height (A): 0.003
Background Pk Height (A)
Date: 12/02/96
0.025
0.023
Mean Cone (ug/L ):
0.01
BD: 0.045
RSD('X) j 317.69
Be
ID: 3956S LCS
Seq. No. : 00047
fl/S Pos. : 15
Date: 12/02/96
uL dispensed: 5 from 0, 5 from 40, 10 from 15
Replicate 1 Time: 19:41
Peak Area
-------
Be
ID;
ft/S Pos.: 16
Date: 12/02/96
uL dispensed: 5 from 40, 5 from 1, 10 from li
Replicate 1 Time:] 19551
Peak ftrea (ft-s): 0.082 Peak Weight (ft): 0.190
Background Pk Area (ft-s) : 0. 143 Background Pk Height (ft) j
Blank Corrected Pk Area (ft-s)s 0. 0a£
Concentration
-------
Recovery is 4. 6"4 (outside of specified limits)
Be IDs 146-4-3ftBCDEX50 Seq. No. : 00052 fl/S Pos. : 18 Date: 12/02/96
uL dispensed: 5 from Cl, 5 from 40, 1® from 18
Be IDs 146-4~2ftBCDX50 Seq. No. : 00053 ft/S Pos. : 16 Date: l£/0£/96
uL dispensed: 5 from 0, 5 from 40, 10 from 16 . «=^, - (
Replicate 1 Time: 20:09
Peak ftrea (ft-s): 0.068 Peak Height (ft): 0.233
Background Pk ftrea (ft-s): 0.123 Background Pk Height (ft): 0.346
Blank Corrected Pk ftrea (ft-s): 0.068
Concentration (ug/L ): 7.65
uL dispensed: 5 from 0, 5 from 40, 10 from 16
Replicate £ (Peak Stored) Time: £0:12
Peak ftrea (ft-s): 0.073 Peak Height (ft): 0.251
Background Pk ftrea (ft-s): 0.131 Background Pk Height (ft): 0.372
Blank Corrected Pk ftrea (ft-s): 0.073
Concentration (ug/L ) : 8. 16
Mean Cone (ug/L ): 7.91 SD: 0.361 RSDC/O: 4.57
Be IDs 146-4-£ftBCDX5ik____Seq. No.: 00054 ft/S Pos.: 16 Date: 12/02/96
— .—.
uL dispensed: 5 from 40, 5 from 1, 10 from 16,
Sample abs. is greater than that of the largest standard.
Replicate 1 TLafe: 28:14
Peak ftrea (ft-s)s 0.100 vf^eak Height (ft): 0.320' -,
Background Pk ftrea (fl-s): 0.163 ^^ Background Pk Height (ft): 0.445
Blank Corrected Pk ftrea (ft-s): 0.
Concentration (ug/L ): 11.23
uL dispensed: 5 from 40, S^rom 1, 18 from 16
Replicate £ (Peak Stored^ Time: £0:16
Peak ftrea (fl-s): 0.097>/ Peak Height (ft): 0.353
Background Pk ftrea (&/€) i 0.159 Background Pk Height (ft): 0.458
Blank Corrected Pk ftrea (ft-s): 0.897
Concentration fi/L ): 11.05 SD: 0.250 RSDC/.): 2. £6
Recovery is r£5^8'/. (outside of specified limits) \}K
'250 tk *«.•<* «* ------------- --------- -----
Be IDs 146-4-£ftBCDX§ef^rt.v
-------
Replicate £ (Peak Stored)
Eeak ftrea. t>SSeq. No. ! 88056 ft/S Pos. s 17 Dates
'-ww-u..-,,,,,.
Be
uL dispensed: 5 'from 40, 5 from 1, IS from 17
Replicate 1 Time: £8:£3
Peak ftrea (ft-s) 5 0.031 Peak Height (ft) s 0.113
Background Pk ftrea
-------
Peak ftrea (ft-s): 0.089 Peak Height (ft): 0.058
Background Pk Area (ft~s): 0.026 Background Pk Height (ft): 0.121
Blank Corrected Pk ftrea (ft-s): 0.009
Concentration (ug/L ): 1.04
uL dispensed! 5 from 0, 5 from 40, 10 from 5
Be IDs CCV=6.0ug/L Seq. No.: 00060 ft/S Pos. : 5 Dates l£/0£/9fe
uL dispensed: 5 from 0, 5 from 40, 10 from 5
Replicate 1 Time: £0:38
Peak ftrea (ft-s): 0.055 Peak Height (ft): 0.330
Background Pk ftrea (ft-s): 0.093 Background Pk Height (ft): 0.44S
Blank Corrected Pk ftrea (ft-s): 0.055
Concentration (ug/L ): 6.20
uL dispensed: 5 from 0, 5 from 40, 10 from 5
Replicate 2 (Peak Stored) Time: £0:40
Peak ftrea (ft-s): 0.056 Peak Height (ft): 0.353
Background Pk ftrea (ft-s): 0.095 Background Pk Height (ft): 0.443
Blank Corrected Pk ftrea (ft-s): 0.056
Concentration : -0.01 SD: 0.023 RSDC/4): 371.53
QC sample is within range -1.0 - 1.8
Be ID: 146-4-3ftBCDEX50 Seq. No. : 00062 ft/S Pos. : IS Date: 12/02/96
uL dispensed: 5 from 0, 5 from 40, 10 from 18
Replicate 1 Time: 20:48
Peak ftrea (A-s): 0.078 Peak Height (ft): 0.338
Background Pk ftrea (ft-s): 0.132 Background Pk Height (ft): 0.432
Blank Corrected Pk flrea (ft-s): 0.078
Concentration (ug/L ): 8,68
175
-------
IIUIU
Replicate £ (Peak Stored) Time: £0;50
§eak Area_, (firsA: 0. 07sS . .- , .->„ Peak Height_,: 3.078
Concentration (ug/L ): 8.70
Mean Cone (ug/L ): 8.69 SD; 0. 0£0 RSD(%); 0.23
Be ID: 146-4-4ABCDX50 Seq. No. : 00063 A/S Pos. : 19 Date: 12/02/96
uL dispensed: 5 from 0, 5 from 40, 10 from 19
Replicate 1 Time: £0:S£
Peak Area : 0. 04fc Peak Height : 0.113 Background Pk Height (A): 0.377
Blank Corrected Pk Area (A-s): 0.064
Concentration (ug/L ) : 7. 12
uL dispensed: 5 from 0, 5 from 40, 10 from 20
Replicate £
-------
Background Pk ftrea (ft-s): 0.100 Background Pk Height (A): 0.389
Blank Corrected Pk Area (A-s); 0.059
Concentration (ug/L ): 6.60
Mean Cone (ug/L ): 6.38 SD; 0.311 RSDC/Os 4.87
Be ID: 146-4-SftBCDE Seq. No. : 00066 ft/S Pos. s 22 Date: 12/02/96
uL dispensed: 5 from 0, S from 40, 10 from £2
Replicate 1 Time: £1:06
Peak ftrea (ft-s): 0.001 Peak Height (ft): 0.004
Background Pk ftrea (A-s): 0.109 Background Pk Height (A): 0.172
Blank Corrected Pk Area (A-s): 0.001
Concentration (ug/L ): 0.12
uL dispensed: 5 from 0, 5 from 40, 10 from ££
Replicate £ (Peak Stored) Time: £1:09
Peak ftrea (fl-s); 0.001 Peak Height (A): 0.005
Background Pk ftrea (ft-s): 0.105 Background Pk Height (ft): 0.144
Blank Corrected Pk ftrea (ft-s): 0.001
Concentration (ug/L ): 0.11
Mean Cone (ug/L ): 0. 12 3D: 0.012 RSD(%): 9.91
Be ID: 146-4-9ftBCDE Seq. No. s 00067 ft/S Pos. : £3 Date: 12/02/96
uL dispensed: 5 from 0, 5 from 40, 10 from £3
Replicate 1 Time: 21:11
Peak Area (ft-s): 0.004 Peak Height (ft): 0.010
Background Pk ftrea (ft-s): 0.099 Background Pk Height (ft): 0.159
Blank Corrected Pk ftrea (ft-s): 0.004 " •„
Concentration (ug/L ): 0.41
uL dispensed: 5 from 0, 5 from 40, 10 from £3
Replicate 2 (Peak Stored) Times 21:14
Peak ftrea (ft-s): 0.003 Peak Height (ft): 0.008
Background Pk ftrea (ft-s): 0.105 Background Pk Height (ft): 0.174
Blank Corrected Pk ftrea (ft-s): 0.003
Concentration (ug/L ): 0.36
Mean Cone (ug/L ): 0.39 SD: 0.041 RSD ('/.): 10.51
Be ID: 146-4-10ftBCDE Seq. No.: 00068 ft/S Pos.: £4 Date: 12/02/96
uL dispensed: 5 from 0, 5 from 40, 10 from £4
Replicate 1 Time: 21:16
Peak ftrea (A-s): 0.001 Peak Height (A): 0.006
Background Pk Area (A-s): 0.058 Background Pk Height (A); 0.156
Blank Corrected Pk Area (A-s): 0.001
Concentration (ug/L ); 0.09
uL dispensed: 5 from 0, 5 from 40, 10 from 24
Replicate 2 (Peak Stored) Time; £1:19
Peak Area (A-s): 0.001 Peak Height (A): 0.006
Background Pk Area (A-s): 0.056 Background Pk Height (A): 0.147
177
-------
wi/t i CWVK=«
Concentration (ug/L ): 0.IS
Mean Cone : 0.218 Background Pk Height : 0.3S5
Blank Corrected Pk Area (A-s): 0.008
Concentration (ug/L ): 0.87
ul_ dispensed: S from 0, 5 from 40, 1@ from 25
Replicate S (Peak Stored) Time: 21:£4
Peak Area ; 0.99 SD: 0.1fe8 RSD (•/.): 16.94
Be ID: 146-4-14ABCD Seq. No. : 00870 A/S Pos. ; £6 Date: l£/0£/96
uL dispensed: 5 from 0, 5 from 40, 10 from S6
Replicate 1 Time: £l:£fe
Peak Area (A-s): 0.007 Peak Height (A): 0.047
Background Pk Area (A-s): 0.174 Background Pk Height
uL dispensed: 5 from 0, 5 from 40, 10 from £6
Replicate £ (Peak Stored) Time: £ls£9
Peak Area (A~s): 0.0"06 Peak Height (A): 0.038
Background Pk Area (A-s): 0.159 Background Pk Height (A): 0.340
Blank Corrected Pk Area (A-s): 0.006
Concentration (ug/L ): 0.69
Mean Cone (ug/L ): 0.75 SD: 0.085 RSD(?O; 11.35
Be ID: 146-4-15ABCD Seq. No. s 0C071 A/S Pos. : £7 Date: l£/8£/96
uL dispensed: 5 from 0, 5 from 40, 10 from £7
Replicate 1 Time: £1:31
Peak Area (A-s): 0.007 Peak Height (A): 0.040
Background Pk Area (A-s): 0.189 Background Pk Height (A): 0.361
Blank Corrected Pk Area (A-s)s 0.007
Concentration (ug/L )s 0.74
uL dispensed: 5 from 0, 5 from 40, 10 from £7
Replicate £ (Peak Stored) Time: £1:34
Peak Area (A-s)s 0.007 Peak Height (A): 0.030
Background Pk Area (ft-s): 0.173 Background Pk Height (A)s 0.£71
Blank Corrected Pk Area (A-s): 0.007
Concentration
-------
Be ID: CCV=6.®ug/L Seq. No.: 00072 A/S Pos. : 5 Dates 12/02/96
uL dispensed! 5 from 0, 5 from 48, 10 from 5
Replicate 1 Time: £1:36
Peak Area (ft-s): 0.059 Peak Height (ft): 0.391
Background Pk Area (A-s): 0,099 Background Pk Height (A): 0.488
Blank Corrected Pk ftrea : 0.495
Blank Corrected Pk Area : 0.015
Blank Corrected Pk Area (A-s): 0.801
Concentration (ug/L ): 0.13
uL dispensed: 5 from 0, 5 from 40, 10 from 8 " -. '
Replicate S (Peak Stored) Time: 21:43
Peak Area (A-s): 0.080 Peak Height (A): 0.003
Background Pk Area (A-s): 0.084 Background Pk Height (A); 8.813
Blank Corrected Pk Area (A-s): 8.008
Concentration (ug/L ): 0.83
Mean Cone (ug/L ): 8.08 SD: 8.873 RSDC/.): 88.77
QC sample is within range -1.8 - 1.0
Be ID: 146-4-17ABCD Seq. No. : 88074 A/S Pos. : 28 Date: 12/02/96
uL dispensed: 5 from 8, 5 from 48, 10 from 28
Replicate 1 Time: £1:46
Peak Area (A-s): 8.068 Peak Height (A): 8.123
Background Pk Area : 8.251
Blank Corrected Pk Area
-------
Mean Cone (ug/L )
7.49
SD: 0.119
RSDCX) : 1.59
Be
IDs 146-4-19ABCD
Seq. No.: 00075
A/S Pos.: £9
Date: 12/02/96
ul_ dispensed: 5 from 0, 5 -from 48, 10 from £9
Replicate 1 Time: £1:50
Peak firea (A-s): 0.06>3 Peak Height : 0.118
Background Pk firea (fl-s): 0.1&4 Background Pk Height : 0.£31
Blank Corrected Pk Area
-------
Replicate 2 (Peak Stored) Time: 22:04
Peak Area (ft-s); 0.063 Peak Height (fl) : 0.285
Background Pk ftrea (fl-s): 0.105 Background Pk Height (ft): 0.397
Blank Corrected Pk flrea
-------
-------
-------
uL dispensed: 5 front 0, 5 from 40, 10 from 31 __ ,_
Replicate £ (Peak Stored) Time: £2:18
Peak ftrea (ft-s): 0.001 Peak Height (ft): 0.003
Background Pk ftrea (A-s): 0.007 Background Pk Height (A): 0.019
Blank Corrected Pk Area (ft-s): 0.001
Concentration ; 0.001 Peak Height (ft): 0.004
Background Pk ftrea (ft-s)s 0.009 Background Pk Height (A): 0.018
Blank Corrected Pk ftrea (ft-s>: 0.001
Concentration (ug/L )s 0.14
Mean Cone
-------
Replicate £ (Peak Stored) Time: £2:32
Peak ftrea (ft-s): 0.001 Peak Height (ft): 0.003
Background Pk ftrea (ft-s): 0.089 Background Pk Height (ft)s 0.01&
Blank Corrected Pk ftrea (fl-s): 0.001
Concentration (ug/L ): 0.10
Mean Cone (ug/L ): 0.08 SD: 0.019 RSD(#): £3.10
Be ID: 146-4-23ftBD6H Seq. No. : 00086 ft/S Pos. : 35 Date: 12/02/96
uL dispensed: 5 from 0, 5 from 40, 10 from 35
Replicate 1 Time: £2:34
Peak ftrea (fl-s): 0.001 Peak Height (ft): 0.003
Background Pk ftrea (ft-s): 0.007 Background Pk Height (ft): 0.022
Blank Corrected Pk ftrea (fl-s): 0.001
Concentration (ug/L ): 0.09
uL dispensed: 5 from 0, 5 from 40, 10 from 35
Replicate £ (Peak Stored) Time: ££:37
Peak ftrea (ft-s): 0.000 Peak Height (ft): 0.003
Background Pk ftrea (ft-s): 0.007 Background Pk Height (ft): 0.018
Blank Corrected Pk ftrea (ft-s): 0.000
Concentration (ug/L ): 0.03
Mean Cone (ug/L ): 0.06 SD: 0.039 RSDC/.); 66. 5£
Be ID: 146-4-23C Seq. No.: 00087 ft/S Pos. : 36 Date: 12/02/96
uL dispensed: 5 from 0, 5 from 40, 10 from 36
Replicate 1 Time: £2:39
Peak ftrea (ft-s): -0.001 Peak Height (ft): 0.003" -.
Background Pk ftrea (ft-s): 0.004 Background Pk Height (ft): 0.014
Blank Corrected Pk ftrea (ft-s): -0.001
Concentration (ug/L ): -0.07
uL dispensed: 5 from 0, 5 from 40, 10 from 36
Replicate 2 (Peak Stored) Time: ££:41
Peak flrea (ft-s): 0.001 Peak Height (ft): 0.003
Background Pk ftrea (ft-s): 0.008 Background Pk Height (ft): 0.015
Blank Corrected Pk ftrea (ft-s): 0.001
Concentration (ug/L ): 0.07
Mean Cone (ug/L ): 0.00 SD: 0.097 RSDC/O: 3343.60
Be ID: CCV=&.0ug/L Seq. No. s 00088 . ft/S Pos. s 5 Date: 12/02/96
uL dispensed: 5 from 0, 5 from 40, 10 from 5
Replicate 1 Time: 2£:44
Peak ftrea (fl-s): 0.060 Peak Height (ft): 0.349
Background Pk ftrea (ft-s)i 0.098 Background Pk Height (ft): 0.447
Blank Corrected Pk Area (fl-s): 0.060
Concentration (ug/L ): 6.76
uL dispensed: 5 from 0, 5 from 40, 10 from 5
Replicate £ (Peak Stored) Time: £2:46
183
-------
Background Pk flrea (fl-s): 0.099 Background Pk Height (ft): 0.397
Blank Corrected Pk ftrea : &.75 SDs 0.004 RSDC54): 0.06
QC sample is within range 4, & - 7. £
Be ID: CCB Seq. No.: 00089 ft/S Pos. : 0 Date: 12/02/96
uL dispensed: 5 from 0, 5 from 40, 10 from 0
Replicate 1 Time: £2:49
Peak firea (fl-s); 0.000 Peak Height (ft): 0.003
Background Pk ftrea : 0.003 Background Pk Height (ft): 0.01£
Blank Corrected Pk flrea (fi-s): 0.001
Concentration (ug/L ): 0.06
uL dispensed: 5 from 0, 5 from 40, 10 from 0
Replicate £ (Peak Stored) Time: £2:51
Peak flrea (fl-s): 0.000 Peak Height (ft): 0.003
Background Pk flrea : 0.000
Concentration (ug/L ): 0.05
Mean Cone (ug/L ): 0.06 SD: 0.010 RSDC/.): 13.16
QC sample is within range -1.0 - 1.0
184
-------
Autosampler Loading Map
Elemefit Files CD.BEL
Loc. Concentration
1 5.0 ug/L
£ 10.0 ug/l
4
5
6
7
a
9
10
11
12
13
14
15
16
17
18
19
£0
£1
££
£3
£4
£5
£6
£7
£8
£9
38
ID/Weight File: EB013. IDW
So 1 ut ions
/ Diluent / ICE
Calib. Blank
stock /-SMI?
Stock / Recovery Stock
ICV=3. Oug/L I-W-MP
CCM=6.0ug/L rll-^r
CHECK LO
39568 MB
39568 LCS
146~4-£ftBCD X10
CCB
146-4-4flBCD X10
146-4-5flBCD X5
146~4-6flBCD X5
146-4-SftBCDE
14&-4-9ABCDE
146-4-10flBCDE
146-4-130BCD
146-4-140BCD
146-4-£lflBCD
146-4-1 1ABCDE
146-4-££fiBCDE
146-4-£3flBDGH
146-4-23C
Modifier 1
185
-------
liiiin-t:Feie: CD.GEL
Print Data: Main+Suppl.
Print; Calib. Curve
Remarks:
STD1: 1-21-3P
STD2: l-£i-4P
ICU: 1-21-5P
CCV: i-Sl-feP
Analyst: HOLSTE
Peak Storage: 1 Repl./Sample
INSTRUMENT: 4100 ZL
Wavelength: 228.S Peak
Signal Type: Zeeman AA
Read Time: 3. O
Sample Replicates: S
Standard Replicates: 2
Technique: HOft Versions 7.30
SI it: 0.7 Low
Signal Measurement: Peak Area
Read Delay: 0.0 BOG Time: £
Spike Replicates: Same as Sample
CALIBRATION:
Solutions ID
Calib. Blank STD. BLANK
Standard 1 STD 1=£. 0ug/L
Standard 2 STD £=5. iZiug/L
Standard 3 STD 3=1®. Oug/L
Reslope Std. 5. 0ug/L
oamp 1 e s
Diluent Location: 0
Modifier #1 Location: 38
Calibration Units: ug/L
Calibration Type: Linear
Cone 1 Location
__._. _., l i7i
£.01 1
5. SI 1
10.01 2
5. 01 1
1.
-
UolumelDiluentl
U o 1 u m e 1
10 5 I
4 111
10 51
10 5 I
10 5 i
10 5 t
Mod i f i er 1
#1 1 #2 1
5 1 I
5 ! i
5 1 1
5 i i
5 1 1
5 1 i
Modifier #2 Location:
Sample Units: ug/L
Furnace Time/Temperature Program:
SteplTemp Ramp Hold Sas Fl ow 1 Read 1 Gas Type 1
1 I 110 1 3d 258 i I Norm 1 ' -, '
2 ! 130 1 35 £50 1
3 1 700 5 £0 £50 1
4 1 140® 0 3 0 !
5 I £50® 1 5 £50 I
1 Norm I
I Norm 1
* 1 Norm 1
1 Norm 1
Injection Temp: £0 Pipette Speed: &5%
Extraction Syst
em: Off
SEQUENCE:
Step Action and Parameters
1 Pi pet diluent +• modifier 1
£ Run HBA steps 1 to End
+• spike +• sample/std
I8r
o
-------
Recalibration Type: Reslope
Locations: None
Cone. Above Calibration fiction: Dilute & Reanalyze After i Rep
Alternate Sample Volumes (uL): 5,2,1
Run Alternate Volume Blanks: Yes
If '/.RSD > 20. 0 and Concentration > .6 then Retry 1 times
Check 54RSD on: Samples + Standards + Spikes + QC Samples
Recovery Measurements:
5 uL of 5 ug/L Standard at Location 1 Gives 2.5 ug/L
Measure Recovery on Samples: 9-10
Add to QC Samples: Yes % Recovery Limits: 75 to 125
QC:
#1 A/S I QC Sample I Cone. Limits I AfterI Periodic I At I Count As!
I Loc. ! ID I Lower Upper ICalibl Check I End I Sample I
1 4 ICV=3.0ug/L £.7 3.3
£ 0 ICE -1.0 1.0
3 5 CCM=6.0ug/L 4.8 7.2 XX
4 0 CCB -1.0 1.0 X X
Run Periodic QC Samples: Every 10
Out of Limit Action: Reslope and Rerun Samples
Matrix Check Calculations:
•/. Difference for Dupls: No Locations:
% Recovery for Spike: No Locations: Cone:
187
-------
_ ^_E.T_.___^T_(.,g
Date: 12/03/96 Time: 09:01 Slits 0.7 L
Data File: EB013.DAT ID/Wt File: EB013.IDW Lamp Current: 0
Technique: HSA Calib. Type: Linear Energy: 60
Remark 1: STD1: 1-21-3P
Remark 2: 8TD2: 1-21-4P
Remark 3: ICV: 1-21-5P
Remark 4: CCV: 1-S1-6P
Cd ID: STD. BLANK Seq. No.: 00001 A/S Pos.: 0 Date: 12/03/96
uL dispensed: 5 from 0, 5 from 38, 10 from 0
Replicate 1 Time: 09:03
Peak Area (A-s): 0.000 Peak Height (fl): 0.008
Background Pk Area (A-s): 0.014 Background Pk Height (A): 0.014
Blank Corrected Pk Area (A-s): 0.001
Concentration (ug/L ): 0.0
uL dispensed: 5 from 0, 5 from 38, 10 from 0
Replicate £' (Peak Stored) Time: 09:06
Peak Area (ft-s): -0.001 Peak Height
-------
Blank Corrected Pk Area (A-s): 0.171
Concentration (ug/L ): 4.5
uL dispensed: 5 from 0, 5 from 38, 10 from 1
Replicate £ (Peak Stored)
Peak flrea (A-s>: 0.Ife9
Background Pk Area (A-s>: 0.030
Blank Corrected Pk flrea (A-s): 0.169
Concentration : 0.81
Cd
ID: STD 3=10.0ug/L
Seq. No.
00004
A/S Pas. :
Date: IE/03/96
uL dispensed; 5 from 0, S from 38, 10 from i
Replicate 1
Peak flrea (fl~s): 0.331
Background Pk flrea (A-s): 0,050
Blank Corrected Pk Area ; 0.33£
Concentration
-------
itiaa - C:\ttJI *
Linear
fl.O
Concentration
»**>. Co**1-: o.»*»0
: 0.033$
10.0
190
-------
Element File: CD. BEL
Dates 12/03/96
Data File: EB813.DftT
Technique
Remark 1:
Remark £:
Remark 3:
Remark 4:
HGfl
STDi : 1-21-3P
STD2: 1-21-4P
ICVi 1-21-5P
CCM: 1-21-6P
Element: Cd
Time: 09:31
ID/Wt File: EB013.IDW
Calib. Type: Linear
Wavelength: 2£8.8
Slit s 0.7 L
Lamp Current: 0
Energy: 60
Cd
ID: ICM=3.0ug/L
Seq. No.: 80005
ft/S Pos. : 4
Dates 12/03/96
uL dispensed: 5 from 0, 5 from 38, 10 from 4
Replicate 1 Time: 09:34
Peak ftrea
-------
Concentration (ug/L ): 1.1
uL dispensed! 5 from 0, 5 from 38, 10 from 6
Replicate S (Peak Stored) Time: 89:47
Peak ftrea (ft-s): 0.037 Peak Height (ft): 8.065
Background Pk Area o . Seq. No.: 00009 A/S Pos. : 8 Date: 12/03/96
"**^-uc,u at .
uL dispensed: 5 from 0, 5 from 38, 10 from 8
Replicate 1 Time: 09:56
Peak Area (ft-s): 0.164 Peak Height : 0.328
Background Pk Area (ft-s): ®. 8£9 Background Pk Height (A): 0.049
Blank Corrected Pk Area (A-s): 0.165
Concentration (ug/L ) : 4. 9
uL dispensed: 5 from 0, 5 from 38, 10 from 8
Replicate £ (Peak Stored) Time: 09:58
Peak Area (A-s): 0.166 Peak Height (A): 0.338
Background Pk Area (ft-s): 0.030 Background Pk Height (A); 0.049
Blank Corrected Pk Area (A-s): 0.166
Concentration (ug/L ): 4.9
Mean Cone (ug/L ): 4.9 SD: 0.04 RSD(%): 0.82
Cd ID: 146-4-£flBCD X10 Seq. No. : 00010 A/S Pos. : 9 Date: l£/03/9fr
uL dispensed; 5 from 0, 5 from 38, 10 from 9
Replicate 1 Time: 10:01
Peak flrea (ft-s): 0.185 Peak Height (A): 0.274
Background Pk Area (ft-s): 0.069 Background Pk Height (ft): 0.061
Blank Corrected Pk ftrea (A-s)5 ®.185
Concentration (ug/L )s 5.5
192
-------
Replicate S (Peak Stored)
Peak Area (fl-s) : 0. 181
Background Pk firea (fl-s>: 0.067
Blank Corrected Pk Area (ft-s) : 0. 181
Concentration : 0.045
Background Pk ftrea (ft-s): 0.044
Blank Corrected Pk ftrea (ft-s): 0.045
Concentration (ug/L ): 1.3
Mean Cone (ug/L ):
Time: 10:15
Peak Height (fl) : 0.094
Background Pk Height (fl): S.037
1. 3
SD: 0.00
RSDCX) : 0. 15
Cd
ID: 146-4-2flBCDX10L
Seq. No.: 00013
ft/S Pos.: 10
Date: 12/03/96
uL dispensed: 5 from 38, 5 from 1, 10 from 10
Replicate 1 Time: 10:18
Peak flrea (ft-s): 0.127 Peak Height (ft): 0.216
Background Pk ftrea (ft-s): 0.054 Background Pk Height (ft): 0.049
Blank Corrected Pk ftrea (fl-s): 0.128
Concentration (ug/L ): 3.8
193
-------
Replicate £ (Peak Stored)
Peak flrea (fl-s) : 0. 128
Background Pk flrea (ft-s): 0.05S
Blank Corrected Pk ftrea (ft-s) : 0. 129
Concentration (u§/L ): 3.8
Mean Cone (ug/L ):
Recovery is 97. &%
3. S
Times 10:21
Peak Height (ft): 0.226
Background Pk Height (ft) s 0.050
SD: 0.0£
RSDC/O : 0.
Cd
ID: 14&-4~3ftBCDEX10
Seq. No.; 00014
fl/S Pos. 5 11
Date; 12/03/96
5.from 38, 10
uL dispensed: 5 TroTn
Replicate 1
Peak Area (ft-s)j 0.368
Background Pk Area (fl-s): 0.092
Blank Corrected Pk flrea (fl-s): 0.369
Concentration (ug/L ); 10.9
•rot
Time: 107^4
Peak Hextjht (A) : 0.534
BackJfround Pk Height (fl)
uL dispensed: 5 from 0, 5 frojuXSS, 10 from 11
Sample abs. is greater thap-^that of the largest standard.
Replicate £ (Peak Store-eD Time: 10: £6
Peak flrea (fl-s): 0. 3JST Peak Height (fl) : 0.559
Background Pk firea/ffi-s): 0.096 Background Pk Height (fl)
Blank Corrected/Pk flrea (fl-s): 0.376
Concentration/fug/L ): 11.1
Sample al
Mean Conc^
is greater than that of the largest standard.
11.0 —-SO: 0. 17
0.097
0.
RSD C/.): 1. 50
Cd
ID: 146-4-4flBCD X10
Seq. No.: 00015
fl/S Pos.: 12
Date: 12/03/96
uL dispensed: 5 from 0, 5 from 38, 10 from 12
Replicate 1 Time: 10:£9
Peak flrea (fl-s): 0.247 Peak Height (fl): 0.406
Background Pk ftrea
-------
.iL spensed: 5 from 0, 5 from 38, 10 from 13
Re icate £ (Peak Stored) Time: 10:38
Pi Area (A-s): 0. £'23 Peak Height (ft): 0. 3£6
B Aground Pk Area (A-s): 0.092 Background Pk Height (A): 0.076
E ank Corrected PN Area (A-s): 0.2£3
Concentration : 0.208
Concentration (ug/L ): 6.1
Mean Cone (ug/L ): 6.2 SDs 0.09 RSDC/.): 1.44
QC sample is within range 4.8 — 7.£
Cd ID: CCB Seq. No. : 00018 A/3 Pos. : 0 • ._Date: 12/03/96
uL dispensed: 5 from 0, 5 from 38, 10 from 0
Replicate 1 Time: 10:46
Peak Area (A-s): 0.000 Peak Height (A): 0.008
Background Pk Area
-------
Blank Corrected Pk Area (A-s): 0.17&
Concentration : 0.174 Peak Height : 0.
Background Pk Area : 0.253
Concentration (ug/L ): 7.5
uL dispensed: 5 from ®, 5 from 38, 10 from 15
Replicate £ (Peak Stored) Time: 11:00
Peak Area (A-s): 0.258 Peak Height (A): 0.317
Background Pk Area (A-s): 0. l&fe Background Pk Height (A): 0. 10S
Blank Corrected Pk Area (A-s): 0.259
Concentration (ug/L >: 7.6
Mean Cone (ug/L ): 7.5 SD: 0.12 RSD(%): l.fcl
Cd ID: 14&-4-9ABCDE Seq. No.: 00021 fi/S Pos. : 16 -...Date: 12/03/96
uL dispensed: 5 from 0, 5 from 38, 10 from 16
Replicate 1 Time: 11:03
Peak Area (A-s): 0.180 Peak Height (A): 0. £75
Background Pk Area (A-s): 0.09& Background Pk Height (A): 0.076
Blank Corrected Pk Area (A-s): 0.180
Concentration (ug/L ): 5.3
uL dispensed: 5 from 0, 5 from 38, 10 from 16
Replicate £ (Peak Stored) Time: 11:06
Peak Area (A-s)s 0.134 Peak Height (A): 0.278
Background Pk Area (A-s): 0.09£ Background Pk Height (A): 0.073
Blank Corrected Pk Area (A-s)s 0.184
Concentration (ug/L ): 5.4
Mean Cone (ug/L ): 5.4 SD: 0.09 RSD(5O: 1.66
Cd IDs 146-4-10ABCDE Seq. No.: 000££ A/S Pos.: 17 Date: 12/03/96
uL dispensed: 5 from 0, 5 from 38, 10 from 17
Replicate 1 Time: 11:09
Peak Area (A-s): 0.£04 Peak Height (A): 0.326
Background Pk Area
-------
ispensed: 5 from 0, 5 from 38, 10 from 17
u!
R .icate £' (Peak Stored)
P « Area (fl-s); 0. £'02
I .:kground Pk flrea (ft—s) : 0. 107
,ank Corrected Pk firea (ft-s): 0. £02
-oncentrat ion
-------
Cd ID: 146-4-15ABCD Seq. No, : 00026 A/S Pos. : 20 Dates 12/0;
uL dispensed: 5 from 8, 5 from 38, 10 from £0
Replicate 1 Time: 11:29
Peak Area (A-s): 0.263 Peak Height (ft): 0.498
Background Pk Area (A-s): 0.053 Background Pk Height (A) s 0.063
Blank Corrected Pk Area : 0.£64
Concentration (ug/L )s 7.8
uL dispensed: 5 from 0f 5 from 38, 10 from 20
Replicate 2 s 0. 1&9
Concentration (ug/L ): 5.0
uL dispensed: 5 from 0, 5 from 38, 10 from 22
Replicate S (Peak Stored) Times 11:43
Peak Area (A-s): 0.167 Peak Height (A): 0.249
Background Pk Area (A-s)s 0.107 Background Pk Height (A): 0.085
Blank Corrected Pk Area (A-s>s 0.167
Concentration (ug/L )s 4.9
Mean Cone (ug/L )s 5.0 SD: 0.05 RSD(*)s 1.00
193
-------
ID: CCV=&.0ug/L
Seq. No.: 00029
ft/S Pos.
Date: 1S/03/96
ul
R-
ispensed: 5 from 0, 5 from 38, 10 from 5
; icate 1
P ,,L( Area (A-s) : 0. 199
F ,ckground Pk ftrea (ft— s) : 0.033
Blank Corrected Pk Area : 0.009
Blank Corrected Pk flrea (ft-s): 0.001
Concentration (ug/L ): 0.0
Peak Height (A): 0.008
Background Pk Height (A): 0.010
uL dispensed: 5 from 0, 5 from 38, 10 from
Replicate S (Peak Stored)
Peak flrea (ft-s): 0.001
Background Pk Area (A-s): 0.007
Blank Corrected Pk Area (fl-s): 0.00£
Concentration (ug/L ): 0.1
Time: 11:54
Peak Height (A): 0.007 • ,
Background Pk Height
-------
I'tean uonc
Cd ID: 14fc-4-llABGDE Seq. No.: 00032 A/S Pos. : 24 Dates 12/0,
uL dispenseds 5 from 0, 5 from 38, 10 from £4
Cd
ID: 146-4-11ABCDE
Seq. No.: 00033
A/S Pos.: £4
Date: 12/03/9
uL dispensed: 5 from 0, 5 from 3S, 10 from 24
Replicate 1 - ... - ••• Timoa-
Peak Area (A-s): 0. £S5
Background Pk Area (A-s): 0.025
Blank Corrected Pk Area (A-s): 0.225
Concentration (ug/L ): fe.7
uL dispensed: 5 from 0, 5 from 3S,
Replicate 2 (Peak Stored)
Peak Area fi-s): 0.131
Concentration (ug/L Jxf 3. 9
Mean Cone (ug/L
Peak HeF&ht (A) i 0.379
Background Pk Height (A)s 0.064
Times 12:06
Peak Height (A): 0.188
Background Pk Height (A): 0.041
RSDC/0 s 37.67
Cd
ID: 146-4-11ABCDE
Seq. No.: 00034
A/S Pos.: £4
Date: 12/83/96
uL dispensed: 5 from 0, 5 .from 38, 10 from 24
Replicate 1 Times 12:09
Peak Area (A-s): 0.129 Peak Height (A): 0.195
Background Pk Area (A-s)s 0.036 Background Pk Height (A):
Blank Corrected Pk Area (A-s): 0.129
Concentration (ug/L ) : 3. S ' •_
uL dispensed: 5 from 0, S from 38, 10 from 24
0. 042
Replicate 2 (Peak Stored)
Peak Area : 0.130
Background Pk Area (A-s): 0.038
Blank Corrected Pk Area (A-s) : 0. 131
Concentration (ug/L ): 3.9
Time: 12:12
Peak Height (A): 0.196
Background Pk Height (A)
0.043
Mean Cone
-------
Me Cone (ug/L ): 4.3 SDs 0,13 RSD<*>: 3.10
D ID: 146-4-12D Seq. No. : 00036 ft/S Pos. : Sfe Dates 12/03/9&
i , dispensed! 5 from 0, 5 from 3fi, 10 from £6
F'.e plicate 1 Time: 1£:£0
Peak Area (A-s): 0.004 Peak Height (A): 0.010
Background Pk Area (A-s): 0.009 Background Pk Height (A): 0.010
Blank Corrected Pk Area : 0.043 Background Pk Height
-------
Cd
ID: 146-4-23C
Seq. No.s 00039
A/S Pos.: 29
Date: IS/03
uL dispensed! 5 from
5 from 38, 10 from £9
Replicate I
Peak Area (A-s)s 0.007
Background Pk Area (A-s): 0.009
Blank Corrected Pk Area (A-s): 0.007
Concentration (Ug/L ): 0.2
Time: 12:37
Peak Height (ft): 0.013
Background Pk Height (A): 0.013
uL dispensed: 5 from 0, 5 from 38, 10 from 29
Replicate 2 ; 0.2
Mean Cone
-------
QC sample is within range —1.0 — 1.0
203
-------
uL dispensed: 5 from 0, 5 from 38f 10 from 11
Replicate 1 Time: 13:03
Peak ftrea (A-s): 0.188 Peak Height (ft): 0.314
Background Pk ftrea (ft~s): 0.045 Background Pk Height (fl) : 0.056
Blank Corrected Pk ftrea (ft-s) : 8. 1S8
Concentration (ug/L ): 5.5
uL dispensed: 5 from 0, 5 from 38, 10 from 11
Replicate 2 (Peak Stored) Time: 13:06
Peak firea (ft-s): 0.185 Peak Height (ft): 0.297
Background Pk ftrea (fl-s): 0.049 Background Pk Height (ft): 0.057
Blank Corrected Pk firea (ft-s): 0.186
Concentration (ug/L ): 5.5
Mean Cone : 0.206 Peak Height (ft): 0.359
Background Pk flrea : 0.037 Background Pk Height (ft): 0.052
Blank Corrected Pk ftrea : 0.001 Peak Height (ft): 0.006
Background Pk ftrea (ft-s)s 0.014 Background Pk Height : 0.014
Blank Corrected Pk firea (ft-s)s 0.002
Concentration (ug/L ): 0,1
Mean Cone (ug/L >: 0.1 SD: 0.00 RSD(*): 3.16
204
-------
205
-------
Cd ID: 146-4-14ABCD X£ Seq. No. : 00045
uL dispensed: 5 from 0, 5 from 38, 10 from 19
Replicate 1 *~
Peak Area (ft-s): 0. 3£3
Background Pk Area (ft-s): 0.096
Blank Corrected Pk Area (A-s): 0.3£3
Concentration (ug/L ): 9.5
A/S Pos.: 19
Date: IS/03/96
i m e~i~y. 3:53
PeakXHeight (A): 0.441
?k ground Pk Height (A): 0. 07 £
uL dispensed: 5 from 0, 5 from
Replicate £ (Peak Stored)
Peak Area (A-s): 0.3£9
Background Pk firea (ft—sX,
Blank Corrected Pk fir
,, 10 from 19
Time: 13:56
0. 099
(A-s): 0.330
Concentration (ug/L/): 9.7
Mean Cone (ug/L ):
9. 6
Peak Height (A): 0.4£3
Background Pk Height (A): 0.071
SD: 0.13
RSDC/.) : 1. 31
Cd
ID: 14&-4-14RBCD X5
Seq. No.: 00047
ft/S Pos.: 19
Date: 12/03/96
uL dispensed: 5 from 0, 5 from 38, 10 from 19
Replicate 1 Time: 14:07
Peak Area
-------
Cd IDs CCB Seq. No. : 80049 A/S Pos. : 0 Date:
uL dispensed! 5 from 0, 5 from 38, 10 from 0
Replicate 1 Time: 14sl8
Peak Area 5 0.001 Peak Heiiht : 0.009
Background Pk Area (A-s): 0.013 Background Pk Height (A): 0, 01S
Blank Corrected Pk Area (A-s>: 0.002
Concentration : 0.009
Background Pk Area (A-s): 0.013 Background Pk Height (A): 0.012
Blank Corrected Pk Area (A-s): 0.002
Concentration : 3. &&
QC sample is within range —1.0 - 1.0
20'
-------
Loc. Concentration
6
7
8
9
10
ii
ia
13
14
15
16
17
18
19
£0
£1
£2
£3
£4
£5
£6
£7
£8
£9
25.13 ug/L
5®. ® ug/L
ID/Weight File: EB014.IDW
Solut ions
Calib. Blank / Diluent / ICB / CCB
Stock i-3»l"tP
Stock / Recovery Stock 1-3^-2. P
ICV=15ug/L |-^\-
CCV=30ug/L r3
CHECK LO
39568 MB
39568 LCS
146-4-£fiBCD X10
14&_4-2fiBCDX10L
146-4-4flBCD XlCi
146-4_5ftBCD X5
146-4-6flBCD X5
146-4-efiBCDE
146-4-9ABCDE
146-4-10ABCDE
i46_4-13ftBCD X5
146-4-14ftBCD
146-4-17ftBCD
146-4-19ABCD
146-4-2 IftBCD
146-4-1 IflBCDE
146-4-12ABCE
146-4-l£D
146-4-23ftBDGH
146-4-23C
Modifier 1
20S
-------
C. 1 t? ill e 11 U r- A A IT • <_»_». wt_ •—
Element: Co
Print Data: Main+Suppl.
Prints Calib. Curve+Elem. Params.
Remarks:
CALIBRATION STDS PREPPED FROM 2-108-4
CHECK STDS PREPPED FROM 2-88-3
Analyst: HOLSTE
Peak Storage: 1 Repl./Sample
INSTRUMENT: 4100 2L
Wavelength: 240.7 Peak
Signal Type: Single Beam
Read Time: 3.0
Sample Replicates: 2
Standard Replicates: 2
Technique: HSfi " Version: 7.3®
Slit: 0.20 Low
Signal Measurement: Peak Area
Read Delay: 0.0 BOC Time: 2
Spike Replicates: Same as Sample
CALIBRATION:
Solut ions
Calib. Blank
Standard 1
Standard 2
Standard 3
Reslope Std.
Samples
Diluent Location: 0
Modifier #1 Location: 40
Calibration Units: ug/L
Calibration Type: Linear
1 ID i
1 t
I t
1 CTA CH AMI/ 1
J ID I 1) cM-HNrs 1 ~"
1STD l=10ug/L 1
I STD 2=25ug/L 1
ISTD 3=50ug/L 1
1 Reslope 50ug/L 1
Cone
10. 0
25.0
50.0
50.0
Locat ion i
i
i
iTl 1
l£l 1
1 1
1 I
2 i
2 1
— 1
u
11
I Molume
10
4
10
10
10
10
Modif i er
#1
Zl
5
#2
Modifier #£ Location:
Sample Units: ug/L
Furnace Time/Temperature Program:
SteplTemp Ramp Hold ISas FlowI Read 1 Gas Type!
1
c*
3
4
5
Inj
!
i
1 1
12
12
ect
110
130
400
400
500
ion
1
1
5
0
1
Temp:
20
25
20
4
5
20
1 250
I 250
1 250
1 0
! 250
Pi
1
I
1
1 *
I
pette
I Norm 1
1 Norm 1
1 Norm i
i Norm 1
I Norm i
Speed: 100"/.
'•
Extraction System: On
SEQUENCE:
Step fiction and Parameters
1 Pipet diluent + modifier 1 •+• spike •+• sample/std
2 Run HSA steps 1 to End
CHECKS:
Recalibration Type:
Locations: None
Reslope
Cone. Above Calibration Action: Dilute & Reanalyze After 1
Alternate Sample Uolumes 20.0
Check %RBD
on:
and Concentration > 5 then Retry
Samples + Standards + Spikes + OC Samples
1 times
Recovery Measurements:
5 uL of 50 ug/L Standard at Location 2 Gives 25.0 ug/L
Measure Recovery on Samples: 9-10
Add to QC Samples: Yes % Recovery Limits? 75 to 1S5
203
-------
#1 ft/S I QC Sample I Cone. Limits IftfterI PeriodicIfit I Count flsl
I Loc. I ID I Lower Upper lCalib'1 Check lEndl Sample I
1 4 ICV=15ug/L 13.5 16.5 X
£ 0 ICB _ -£.0 £. "3 X
3 5 CCV=30ug/L £4.0 3&.0 X X
4 0 CCB -2.0 £.0 "" XX
Run Periodic QC Samples: Every 10
Out of Limit fiction: Reslope and Rerun Samples
Matrix Chech Calculations:
"/. Difference for Dupls: No Locations:
'/- Recovery for Spike: No Locations: Cone:
210
-------
Element File: CO.GEL
Date; 12/03/9S
Data File: EB014.DAT
Element: Co
Time; 15;32
ID/Wt File: EB014.IDW
Technique: HGfi Calib. Type: Linear
Remark 1: CALIBRATION STDS PREPPED FROM £-108-4
Remark 2: CHECK STDS PREPPED FROM £-88-3
Wavelength: £40.7
SI it i 0. £@ L
Lamp Current:
Energy : 57
0
Co
ID: STB BLANK
Seq. No.: 0300£
fl/S Pos. : 0
Date: l£/03/96
uL dispensed: 5 from 0, b from 40, Id from 0
Replicate 1 Time: 15:34
Peak firea (A-s>: 0.003 Peak Height (ft)
Blank Corrected Pk Area (A-s): -0.000
Concentration (ug/L ) : -0. 1
0, 089
uL dispensed: 5 from 0, 5 from 40, 10 from 0
Replicate £ (Peak Stored) Time: 15:36
Peak flrea (A-s): 0.003 Peak Height (ft): 0.011
Blank Corrected Pk flrea (A-s): -0.000
Concentration (ug/L ) : —0. 1
Mean Cone (ug/L ) :
Auto-zero performed.
-0. 1
SD: 0.01
RSDC/.) : 15.06
Co
ID: STD l=10ug/L
Seq. No.: 00003
fl/S Pos.: 1
Date: 12/03/96
uL dispensed: 11 from 0, 5 from 4®, 4 from 1
Replicate 1 Time: 15:39
Peak flrea (A-s): 0.036
Blank Corrected Pk flrea (A-s): 0.033
Concentration (ug/L ): 13.6
Peak Height (A): 0.07£
uL dispensed: 11 from 0f 5 from 40, 4 from 1
Replicate £ (Peak Stored)
Peak Area (A-s): 0.035
Blank Corrected Pk flrea (A-s): 0.03£
Concentration (ug/L ): 13.0
Mean Cone (ug/L )s
13.
Standard number 1 applied. C10.03
Correlation coefficient: 1.00000
Time: 15:41
Peak Height (A): 0.068
SD: 0.4£
Slope: 0.0033
RSDC/t) : 3. £0
Co
ID: STD £=£5ug/L
Seq. No.: 00004
A/S Pos.: 1
Date: 1£703/96
uL dispensed: 5 from 0, 5 from 40, 10 from 1
Replicate 1 Time: 15:44
Peak Area (A-s): 0.079 Peak Height (A): 0.138
Blank Corrected Pk flrea (fl-s): 0.076
Concentration (ug/L )5 £3.3
uL dispensed: 5 from 0, 5 from 40, 10 from 1
Replicate £ (Peak Stored) Time: 15:46
Peak Area (A-s): 0.079 Peak Height (A): 0.143
211
-------
Concentration (ug/L ): £3.4
Mean Cone : 8.152 Peak Height (ft): 0.£31
Blank Corrected Pk ftrea Cft-s) : 0. 149
Concentration (ug/L ): 43.£
uL dispensed; 5 from 0, 5 from 40, 10 from £
Replicate £ (Peak Stored)
Peak ftrea (ft-s) : 0. 151
Blank Corrected Pk Area (A-s); 0,143
Concentration (ug/L ): 47,9
Mean Cone (ug/L
48. 1
Standard number 3 applied. C50.03
Correlation coefficient: B, 999£0
lime; 15:51
Peak Height (ft): 0.£36
SD: 0.£0
Slopes 0.0030
RSDC/-) : 0. 41
{Display Calibration - C;\ftft_U|*
Linear
Corr.
Sloe-a:
C.9
212
-------
Element File: CO.GEL
Date: 12/03/96
Data File: EB014.DAT
Technique: HGA
Element : Co
Time: 15:53
ID/Wt File: EB014.IDW
Calib. Type: Linear
Wavelength: £40.7
Slit: C.£8 L
Lamp Current : 30
Energy: 57
Remark 1: CALIBRATION STDS PREPPED FROM £-100-4
Remark £: CHECK STDS PREPPED FROM 2-SS-3
Co
ID: ICV=15ug/L
Seq. No.: 00006
ft/S Pos. : 4
Uate: 12/83/9&
uL dispensed: 5 from 0, 5 from 40, 10 from 4
Replicate 1 Time: 15:55
Peak Area (A-s): 0.05£ Peak Height (A): 0.093
Blank Corrected Pk flrea (A-s): 0.849
Concentration (ug/L ); 16.4
uL dispensed: 5 from 8, 5 from 40, 10 from 4
Replicate £ (Peak Stored) Time: 15:58
Peak Area (A-s): 0.051 Peak Height (ft): 0.095
Blank Corrected Pk Area (A-s): 0.048
Concentration (ug/'L ): 15.9
Mean Cone (ug/L ) : 16. £ SD: 0.34
QC sample is within range 13.5 - 16.5
RSDC/.) : £.11
*V ""V Ar AJP fv A# *V A.' *V A^ *"\t rv A/ AJ *V A^ A* A* AP A* *V A.- *V '"w 'V r« *\c A* **t/ 'v *V A^ A^ *"^ *V r\f f\; f
/ AT A* A/ A.*
A/ A/ A.- Aj A- A/
Co
ID: ICB
Seq. No.: 00007
ft/S
0
uL dispensed: 5 from 0, 5 from 48, 10 from 0
Replicate 1 Time: 16:00
Peak flrea (A-s): 0. 00£ Peak Height (ft)
Blank Corrected Pk Area (A-s): -0.001
Concentration (ug/L ): -0.4
uL dispensed: 5 from 0, 5 from 40, 10 from ®
0.
Replicate £ (Peak Stored)
Peak Area (A-s): 0.882
Blank Corrected Pk Area (A-s): -8.881
Concentration (ug/'L ): -0.3
Mean Cone (ug/L ): -8.3
QC sample is within range —£.0 — £.0
Time: 16:02
Peak Height (A)
SD: 0.05
0.013
Date: i£/03/96
RSDC/.) : 14. 36
Co
ID: CHECK LO
Seq. No.: 0000S
A/S Pos.
6
uL dispensed: 5 from 0, 5 from 4®, 10 from 6
Replicate 1 Time: 16:05
Peak Area (A-s): 0.005 Peak Height (A): 0.014
Blank Corrected Pk Area (A-s): 8.802
Concentration (ug/L ): 0.7
uL dispensed: 5 from 0, 5 from 40, 10 from 6
Replicate £ (Peak Stored) Time: 16:07
Peak Area (A-s): 0.087 Peak Height (A): 0.018
Blank Corrected Pk Area (A-s): 0.884
Date: 12/03/96
213
-------
Mean Cone
-------
Replicate 1
Peak Area (A-s)
Blank Corrected Pk Area (A-s): 0.172
Concentration (ug/L ): 57.4
: j. ci i w *= xt v ^v m i * w K* i '
Time: 16:26
Peak Height . : 0. 87
Co
ID; 146-4-£ABCDXl-€tPDS Seq. No. : 00014
A/S Pos. : 10
uL dispensed: 5 from 40, 5 from 2, 10 from 10
Replicate 1 Time: 16:36
Peak Area (A-s): 0.085 Peak Height
Blank Corrected Pk Area (A-s): 0.082
Concentration (ug/L ); 27.5
uL dispensed: 5 from 40, 5 from £, 10 from 10
Replicate £ (Peak Stored)
Peak Area (fi-s): 0.085 -
Blank Corrected Pk Area (A-s): 0.082
Concentration (ug/L >: £7.5
Mean Cone s f 20.6 3D: 1.18 RSD <•/.): 5. 7*i
Co ID: 146-4-4ABCD X10 Seq. No.: 00016 ft/S Pos. : 12 Date: 12/0,i/9&
uL dispensed: 5 from 0, 5 from 48, 10 from IS
Replicate 1 Time: 16:46
Peak Area (ft~s): 0.078 Peak Height (ft): 0.182
Blank Corrected Pk flrea (ft-s): 0.075
Concentration
-------
Co
ID: CCV=30ug/L
Seq. No.: 00019
ft/S Pos. : 5
Date: 12/03/96
uL dispensed: 5 from ®, 5 from 40, 10 from 5
Replicate 1 Time: 16:58
Peak flrea (ft-s): 0, 892
Blank Corrected Pk Area : 30.0 SD: 0.19
QC sample is within range 24.0 — 36.0
RSDC/0 : 0.65
Co
ID: CCB
Seq. Mo.: 80020
ft/S Pos. : 0
uL dispensed: 5 from 0, 5 from 40, 10 from 0
Replicate 1 Time: 17:03
Peak ftrea (ft-s): 0.004 Peak Height
Blank Corrected Pk flrea (fl~s): 0.001
Concentration (ug/L ): 0.2
0. 026
uL dispensed: tj from 0, 5 from 40, 10 from 0
Replicate 2 (Peak Stored) ' Time: 17:06
Peak Area (A-s): 0.004 Peak Height (ft): 0.024
Blank Corrected Pk ftrea (ft-s): 0.001
Concentration (ug/L ): 0.3
Mean Cone (ug/L ) : 0.3
QC sample is within range -2.0 - 2.0
SD: 0.09
Date: 12/03/96
RSDC/O : 32.05
Co
ID: 146-4-6ftBCD X5
Seq. No.: 00021
ft/S Pos. : 14
uL dispensed: 5 from 0, 5 from 40, 10 from 14
Sample abs. is greater .than that of the largest standard.
Replicate 1 Time: 17508
Peak ftrea (ft-s): 0.176 Peak Height
-------
Blank Corrected Pk Area (A-s): 0.094
Concentration (ug/L ): 31.3 Correct-ed Cone (ug/L ): 6£. 7
Mean Cone (ug/L >: 31.1 SD ; 0.26 RSDC/.): @, 85
Corrected Cone Cug/L ): 62.3
Co ID: 14fe-4-8ABCDE Seq. No.: ©0023 A/S Pos. : 15 Date: l£/w3/9£-
uL dispensed: ,S_ from 0, 5 from 40, 10 from 1
Replicate 1 "
Peak Area : 0.142 Peak Height (A): 0.£4S
Blank Corrected Pk Area (A-s): 0.139
Concentration (ug/L ): 46.5
uL dispensed: 5 from 0, 5 from 40, 10 from 15
Replicate £ (Peak Stored) Time: 17:23
Peak Area
-------
seq. No. :
MOE.: l/
Date;
uL dispensed: 5 from 3, 5 from 4®, 1® from 17
Replicate 1 Timei 17:3®
Peak ftrea
Co
ID: 146-4-13flBCD
fl/S Pos.: IS
Dates 12/03/96
uL dispensed: 13 from 0, 5 from 40, £ from IS
Replicate 1
Peak flrea (fl-s); 0.079
Blank Corrected PN flrea e^a (fl-s)
Concentration (ug/L/): £'7.8
0.076
Time:
PealvWeight (ft) : 0. 199
Corrected Cone
-------
Replicate 1 Time: 17:45
Peak Area (A-s)s 0. 1S6 Peak He-ight -(A): 0.320
Blank Corrected Pk flrea |