o-EPA
United States Industrial Environmental Research EPA-600/7-79-015c
Environmental Protection Laboratory February 1979
Agency Research Triangle Park NC 27711
Application of
Combustion Modifications
to Industrial Combustion
Equipment
(Data Supplement B)
Interagency
Energy/Environment
R&D Program Report
-------
RESEARCH REPORTING SERIES
Research reports of the Office of Research and Development, U.S. Environmental
Protection Agency, have been grouped into nine series. These nine broad cate-
gories were established to facilitate further development and application of en-
vironmental technology. Elimination of traditional grouping was consciously
planned to foster technology transfer and a maximum interface in related fields.
The nine series are:
1. Environmental Health Effects Research
2. Environmental Protection Technology
3. Ecological Research
4. Environmental Monitoring
5. Socioeconomic Environmental Studies
6. Scientific and Technical Assessment Reports (STAR)
7. Interagency Energy-Environment Research and Development
8. "Special" Reports
9. Miscellaneous Reports
•
This report has been assigned to the INTERAGENCY ENERGY-ENVIRONMENT
RESEARCH AND DEVELOPMENT series. Reports in this series result from the
effort funded under the 17-agency Federal Energy/Environment Research and
Development Program. These studies relate to EPA's mission to protect the public
health and welfare from adverse effects of pollutants associated with energy sys-
tems. The goal of the Program is to assure the rapid development of domestic
energy supplies in an environmentally-compatible manner by providing the nec-
essary environmental data and control technology. Investigations include analy-
ses of the transport of energy-related pollutants and their health and ecological
effects; assessments of, and development of, control technologies for energy
systems; and integrated assessments of a wide range of energy-related environ-
mental issues.
EPA REVIEW NOTICE
This report has been reviewed by the participating Federal Agencies, and approved
for publication. Approval does not signify that the contents necessarily reflect
the views and policies of the Government, nor does mention of trade names or
commercial products constitute endorsement or recommendation for use.
This document is available to the public through the National Technical Informa-
tion Service, Springfield, Virginia 22161.
-------
EPA-600/7-79-015c
February 1979
Application of Combustion
Modifications to Industrial
Combustion Equipment
(Data Supplement B)
by
K.T. Fisher, H.J. Buening, W.A. Carter,
P.K. Engel, S.C. Hunter, and R.J. Tidona
KVB, Inc.
17332 Irvine Boulevard
Tustin, California 92680
Contract No. 68-02-2144
Program Element No. EHE624A
EPA Project Officer: Robert E. Hall
Industrial Environmental Research Laboratory
Office of Energy, Minerals, and Industry
Research Triangle Park, NC 27711
.Prepared for
U.S. ENVIRONMENTAL PROTECTION AGENCY
Office of Research and Development
Washington, DC 20460
-------
.-' '.'.'• Limitations On Application Of Data Reported
The data cited in this report are test results for measured pollutant
emissions from a wide variety of industrial combustion equipment types. Only
a limited number of each equipment type could be tested. Therefore, these
emission levels are not suitable for use in estimating mean .emissions from
industrial combustion .equipment classes and should hot be used alone in
compiling area-wide emission inventories. Also, they are hot suitable for
predicting emissions from any one process or as regulatory limits or emission
standards: Use of these emissions as emission standards may place a large
proportion1of the industrial combustion device population in noncompliance.
The data can however be of use in supplementing other data used for these
purposes. The purpose of this test program was to investigate the feasibility
of combustion modifications for emissions control) not to develop a compre-
hensive emissions data base. '
Suppl. B ii
-------
CONTENTS
Page
FOREWORD iv
INSTRUMENTATION vii
GLOSSARY viii
CONVERSION FACTORS : ix
SITE LOCATION NUMBER
Data Supplement B
10/1 Wood-Bark Boiler 491
10/2 Black Liquor Recovery Boiler 525
11 Carbon Monoxide Boiler 599
12/1 Petroleum, Process Heater 624
12/2 Petroleum Process Heater 645
13 Wood-Bark Boiler 690
14 Open Hearth Furnace 763
... , 15 . Diesel Engine , 820
16/1 Steel Billet Reheat Furnace 891
16/2 Steel Ingot Soaking Pit 914
Data^ Supplement A contains the following location numbers:
1 Ceramic Tunnel Kiln 1
2 Internal Combustion Engine 10
3 Rotary Kiln 36
4 Petroleum Refinery Heater 58
5/1 Process Heater 136
5/2 Process Heater ; 178
6 Aluminum Melting Furnace 216
7/1 Petroleum Process Heater 225
7/2 Petroleum Process Heater 275
7/3 Gas Turbine Combined Cycle 303
8 Gas Turbine Combined Cycle 338
9 Rotary Kiln 387
Suppl. B iii
-------
FOREWORD
The purpose of this Data Supplement, which is presented in two volumes,
is to document data in greater detail than was practical in the final report
for this contract. It is intended to provide the necessary details to other
researchers who are interested in performing their own analysis.
Readers are referred to the contract final report for information
as to objectives, selection of units, measurement procedures, interpretations
and conclusions.1
All data presented for gaseous emission concentrations of NO, NO ,
CO, HC, SO- and SO, are expressed in parts per million by volume (ppm) on
a dry basis corrected to 3 percent 0_ by volume (dry), in the flue gas.
The data are arranged in this volume by Location Number for Locations
1 through 16. A location is defined as one company or plant in which one or
more units were tested. Each unit tested at a location is identified by a
unit number. The contract final report refers to the test number when data
are discussed. The test number is of the form xx/yy-zz, where xx = location
number, yy = unit number, and zz = test number on that unit. For sites where
only one unit was tested the /yy unit number is deleted.
1Hunter, S. C., et al., "Application of Combustion Modifications to Industrial
Combustion Equipment," EPA 600/7-79-105a, January 1979.
Suppl. B iv
-------
For each unit tested, the data supplement contains the following
information:
1. Equipment Design Data
Design data tabulations include: unit description, installation
date, process capacity, burner description, fuels burned, combus-
tion air temperature and other data pertinent to each unit.
'.2. Mobile Laboratory Data (Emission Measurements)
Emission measurements tabulated for each test include test number,
test load, combustion conditions (excess 02, CC>2), gaseous emis-
sions (NOX, NO, CO, HC, SOX and SO2 all at 3% O2, dry), total
particulates and solid (filterable) particulates, thermal
efficiency, Bacharach smoke spot number, and plume opacity.
3. Operating Data
Data pertinent to the process is tabulated for each test. v
4. Fuel Analyses
Analyses of test fuels are included as reported for fuel samples
collected during tests.
5. Particulates Measurement Data
Particulates data includes measurements! of total and solid
particulates by EPA Method 5.
6. Cascade Impactor Data
Impactor data include impactor flow conditions, stage collection
weights, and calculated aerodynamic particle size for each stage.
One impactor used was a Brink Model B (BMS-11) with the following
stage dimensions:
Spacing of
Jet No. Jet Dia., in^ Jet Opening, in.
0.747
0.533
0.419
0.282
0.220
1
2
3
4
5
0.249
0.1775
0.1396
0.0946
0.0731
Suppl. B
-------
The second impactor used was an Anderson 2000 Mark III with
the following stage dimensions:
Stage No. Jet Diameter, cm :
1 0.1638
2 ,0.1253
3 0.0948
4 0.0759
5 0.0567 , .
6 0.0359
7 0.0261 :
8 . 0.0251
7. Opacity Data
Plume opacity was observed by EPA Method 9.
8. Stack Traverse Data
Stack traverses are made with a pitot tube. ;
9. Trace Species and Organics Sample Data
Sample acquisition logs and results of sample analyses by
atomic absorption, "spark source mass spectrometry, wet
chemistry, gas chromatography, and gas chromatography/mass
spectrometry are included.
Dash marks entered on the data forms indicate that data were not
available.
Suppl. B vi
-------
. INSTRUMENTATION
The emission measurements were made with. instrumentation contained in
a 2.5 by 9 meter (8 by 27 ft) laboratory trailer. The gaseous emission
measurements were made with analyzers located in the measurement console in
the trailer. The particulate concentration, particulate size, sulfur oxides,
and trace species concentration measurements were made with instrumentation
prepared in the wet chemistry area of the laboratory and taken to the sample
port. The weighing and titration were done in or near the laboratory.
The emission measurement instrumentation used for the program was
that shown in Table 1. The operation of the instrumentation is discussed
in detail in the contract final report.
TABLE 1. EMISSION MEASUREMENT INSTRUMENTATION
Emission
Symbol
Measurement Method
Equipment Mfgr & Model
Nitric oxide
Oxides of nitrogen
Carbon monoxide
Carbon dioxide
Oxygen
Hydrocarbons
Sulfur dioxide
Sulfur dioxide
and trioxide
Total particulate
matter
Particulate size
Smoke spot
Opacity
Trace Species
and Organics
NO
CO
co2
0.
HC
SO.
S°2
80,
PM
TS&O
Chemiluminescent*
Chemiluminescent*
Spectrometer*
Spectrometer*
Polarographic*
Flame ionization*
Photometric*
Absorption/
titration
EPA Std. Method 5
Cascade impactor
Reflection
EPA Std. Method 9
EPA SASS Train
Thermo Electron, 10A
Thermo Electron, 10A
Beckman, 864
Beckman, 865
Teledyne, 326A
Beckman, 402
Dupont 400
KVB Equipment Co.
Joy Mfg. Co.
Monsanto~Brink, B(BMS-11)
Anderson 2000, Mark III
Research Appliance Co.
Acurex/Aerotherm SASS
*Precision, +_ 1% of Full Scale
Suppl. B
vii
-------
GLOSSARY OF SYMBOLS ~USED ON DATA FORMS
burner Type
Air
' ChGrt
Piilv.
Ring
SpStk
Spud
Steam
Test Type
Air Reg
Atom Press
BOOS
Base
BrTune
CombCyc
Damper
HiAir
HiLoad
LowAir
LowLoad
LowNOx
NrmlAir
OFA
.SCA
SnglCyc
Steamlnjec
VPH
Viscosity
Air Atomizer
Chain Grate
Puilverizer
Natural Gas Ring
Spreader Stoker
Natural Gas Gun
Steam Atomizer '•
Test Fuel
Coal
NG
Ref.Gas
NG/#6
#2
#5
#6
PS300
Air Register Adjustment
Burner Atomizing Pressure Adjustment
Burners Out Of Service
Baseline
Boiler Tuneup
Combined Cycle
Air Damper Adjustment
High Excess Air
High Load
Low Excess Air
Low Load
Low NOx Condition
1 Normal Excess Air
Overfire Air
Staged Combustion Air
Single Cycle
Steam Injection
Variable Combustion Air Temperature
Fuel Oil Viscosity
Coal
Natural Gas
Refinery Gas
Mixture, NG and #6
'•:•<
No. 2 Grade Fuel Oil
No. 5 Grade Fuel Oil
No. 6 Grade Fuel 6il
Pacific Standard Fuel
Oil No. 300
Suppl. B
Vlll
-------
CO
I
. H-
X
CONVERSION FACTORS
SI Units to Metric or English Units
To Obtain ppm
*These conversions depend on fuel composition.
The values given are for typical fuels.
Multiply*
Concentration
To Obtain
g/Mcal
106 Btu
Btu
lb/106 Btu
ft
in.
ft2
ft3
Ib
Fahrenheit
Fahrenheit
psig
psia
iwg (39.2 °F)
6
10 Btu/hr
GJ/hr
From
ng/J -
GJ
gm cal
ng/J
m
cm
2
m
m
kg
Celsius
Kelvin
Pa
Pa
Pa
.MW
MW
Multiply By
0.004186
.0.948
3.9685xlO~~3
0.00233
3.281
0.3937
10.764
35.314
2.205
tp = 9/5 (tc) +32
t_ =.1.8^ - 460
•F K
P . = .(P ).(1.450xlO~Vl4,7
psig pa
P . = (P ) (1.450x10 )
nci-j * ria
f oid . k*** *>
P. = (P ) (4.014x10 )
iwg pa
3.413
3.60
at 3% O^ of
"Natural Gas Fuel
CO
HC
NO or NO
x
SO., or SO
2 x
Oil Fuel
CO
HC
NO or NO
x
SO_ or SO
2 x
Coal Fuel
CO
HC
NO or NO
x
SO_ or SO
2 x
in ng/J by
3.23
5.65
1.96
1.41
2.93
5.13
1 . 78
1.28
2.69
4.69
1.64
1.18
-------
CO
•a
?.
® To Obtain
ng/J
ng/J
GJ
m
cm
m2
m3
kg
Celsius
Kelvin
Pa
Pa
Pa
MW
MW
English and Metric Units to SI Units
From
lb/106 Btu
g/Mcal .
106 Btu
ft
in.
ft2
ft3
Ib
Fahrenheit
Fahrenheit
psig
psia
iwg (39.2 ?F)
106 Btu/hr
GJ/hr
Multiply By
430
239
1.055
0.3048
2.54
0.0929
0.02832
0.4536
tc = 5/9 (tp - 32)
t_ - 5/9
-------
WOOD-BARK BOILER
Location No . » O _ . _ Unit No.
Unit Description ^/cx _ 't)*JR.KL l6oV LC£.
Installation Date
Heater Rating
Burner Description O^-lQ 4- Sv.aTT£i"P "TaP-oAT MocfiSpOD CrfA
I \ "Tj I I 1 x-—'
Test Fuel Combinations VJoovgTXeXlC, Kj \T • g»
Fuel Temp, at Burner (°F)
Primary Air Temp. (°F) OkM^-fecStE.Arre g 14^ -.5^5°
Comments:
Suppl. B 491
-------
Test No.
Unit No.
MOBILE LABORATORY DATA
Date g-/7-?6 Location
Capacity
10
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6. Flue Diam. or- Size, ft
T. Probe Position g ' t* ®
8. Oxygen (%)
9. NOx (hot) read/3% 02 (ppm)
10. NO (hot) read/3% 02 (ppm)
11. N03 (hot) read/3% 02 (ppro)
12. NO (cold) read/3% 02 (ppm)
13. Carbon Dioxide (%)
14. Carbon Monoxide (ppm) uncor/cor
15. Hydrocarbon (ppm) uncor/cor
16. Sulfur Dioxide (ppm) uncor/cor
17. Smoke Spot (Bacharach)
18. Atmos. Temp. (CF/°C)
19. Dew Point Temp. (eF/eC)
20. Atroos. Pressure (in. Hg)
21. Relative Humidity (%)
22.
23.
24.
25.
26.
27.
28.
29.
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Data Sheet 6002-2
492
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Test No. fOJI - I
Unit No. '
MOBILE LABORATORY DATA
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11. NO? (hot) read/3% 02 (ppm)
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13. Carbon Dioxide (%)
14. Carbon Monoxide (ppm) uncor/cor
15. Hydrocarbon (ppm)
16. Sulfur Dioxide (ppm)
17. Smoke Spot (Bacharach)
18. Atmos. Temp. (cF/eC)
19. Dew Point Temp. (°F/<>C)
20. Atmos. Pressure (in. Hg)
21. Relative Humidity (%)
22.
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Test No./O//- /
Jnit No. I
MOBILE LABORATORY DATA
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Fuel M d .i
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10. NO (hot) read/3% 02 (ppm)
11. NOj (hot) read/3% 02 (ppm)
12. NO (cold) read/3% 02 (ppm)
13. Carbon Dioxide (%)
14. Carbon Monoxide (ppm) uncor/cor
15. Hydrocarbon (ppm) uncor/cor
16. Sulfur Dioxide (ppm) uncor/cor
17. Smoke Spot (Bacharach)
18. Atmos. Temp. (eF/eC)
19. Dew Point Temp. (DF/°C)
20. Atmos. Pressure (in. Hg)
21. Relative Humidity (%)
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-------
MOBILE LABORATORY DATA .
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Unit No. / FuelfJ.Q. +UooJ Capacity '
Test No.
__ Engr. //4A/.S
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2. Date .
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10. NO (hot) read/3% 02 (ppm)
11. NO^Jhot) read/3% Oz (ppm)
12. NO (cold) read/3% 02 (ppm) .
13. Carbon Dioxide (%)
14. Carbon Monoxide (ppm) uncor/cor
15. Hydrocarbon (ppm)
16. Sulfur Dioxide, (ppm)
17. Smoke. Spot (Bacharach)
18. Atmos. Temp. . (eF/°C)
19. Dew Point Temp. (°P/8C)
20. Atraoe. Pressure (in. Hg)
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MOBILE -LABORATORY DATA
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10. NO (hot) read/3% 02 (ppm)
11. NO? (hot) re ad/ 3% 02 (ppm)
12. NO (cold) read/3% 02 (ppm)
13. Carbon Dioxide (%)
14. Carbon Monoxide (ppm) uncor/cor
15. Hydrocarbon (ppm)
16. Sulfur Dioxide (ppm)
17. Smoke Spot (Bacharach)
18. Atmos. Temp. (°F/°C)
19. Dew Point Temp. (°F/0C)
20. Atmos. Pressure (in. Hg)
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Test No.
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MOBILE LABORATORY DATA
£•?£ Location _ / $
Test No.
Engr.
^dgaW^ Capacity
Unit Type
4 <
Burner Type
1. Test No.
2. Date
3. Time
4. Load
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6. Flue Diam. or Size, ft
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8. Oxygen (%)
9. NOx (hot) read/3% 02 (ppm)
10. NO (hot) read/3% 02 (ppm)
11. NO? (hot) re ad/ 3% 02 (ppm)
12. NO (cold) read/3% 02 (ppm)
13. Carbon Dioxide (%)
14. Carbon Monoxide (ppm) uncor/cor
15. Hydrocarbon (ppm)
16. Sulfur Dioxide (ppm)
17. Smoke Spot (Bacharach)
18. Atnos. Temp. (eF/eC)
19. Dew Point Temp. (eF/eC)
20. Atmos. Pressure (in. Hg)
21. Relative Humidity (%)
22.
23.
24.
25.
26.
27.
28.
29.
30.
/0/-2.
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6002-2
498
-------
Test No.
Unit No.
~ X Date
FuelA'.g.
Unit Type
& £ /e./>r£-
1. Test No.
2. Date
3. Time
4. Load
5. Process Rate
6. Flue Diam. or Size, ft
7. Probe Position
8. Oxygen (%)
9. NOx (hot) read/ 3% 03 (ppm)
10. NO (hot) read/3% 02 (ppm)
11. NO? (hot) read/3% 02 (ppm)
12. NO (cold) read/3% 02 (ppm)
13. Carbon Dioxide (%)
14. Carbon Monoxide (ppm) uncor/cor
15. Hydrocarbon (ppm)
16. Sulfur Dioxide (ppm)
17. Smoke Spot (Bacharach)
18. Atnos. Temp. (°F/eC)
19. Dew Point Temp. (eF/°C)
20. Atmos. Pressure (in. Hg)
21. Relative Humidity (%)
22.
23.
24.
25.
26.
27.
28.
29.
30.
ID//- ^-
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Data Sheet 6002-2
II
409
-------
AU6 24676
Test No.
Unit No.
Date
/
Fuel
Unit Type
ec?
MOBILE LABORATORY DATA
/X".
CX
Capacity
Burner Type
Test No.
Engr._
1. Test No.
2. Date
3. Time
4. Load
5. Process Rate
6. Flue Diam. or Size, ft
7. Probe Position
8. Oxygen (%_)
9. NOx (hot) read/3% 02 (ppm)
10. NO (hot) read/3% 02 (ppm)
11. NO? (hot) read/3% 02 (ppm)
12. NO (cold) read/3% 02 (ppm)
13. Carbon Dioxide (%)
14. Carbon Monoxide (ppm) uncor/cor
15. Hydrocarbon (ppm)
16. Sulfur Dioxide (ppm)
17. Smoke Spot (Bacharach)
18. Atmos. Temp. ('F/°C)
19. Dew Point Temp. (eF/"C)
20. Atmos. Pressure (in. Hg)
21. Relative Humidity (%)
22.
23.
24.
25.
26.
27.
28.
29.
30.
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Data Sheet 6002-2
-------
OPERATING DATA
Location 10
Unit 1
<2>
Test Ho.
Date
Time
Steam Plow, Ib/hr * 10'
Steam Outlet Press., psig
Steam Outlet Temp. , °F
Burner Gas Press. , psig
Furnace Draft, in. H.,0
Main Undergrate Air Press., in. H,O
Primary Air Press., in. H.,0
A.H. Air Outlet Press., in. H.,0
A.H. Air Inlet Press., in. H.,0
P.O. Pan Discharge Press., in. H.,0
Low. Over fire Air Press., in. H.,0
Up. Over fire Air Press., in. H,0
I.D. Fan Inlet Draft, in. H.,0 '
A.H. Gas Out, in. H,0
Boiler Outlet Draft, in. H.,0
Undergrate Air Flow, percent
Hood Steam Flow, percent
Windbox Air Flow, percent
Total Air Flow, percent
Gas Flow to Burners, SCFH
Boiler Outlet 0.,, percent
Boiler Outlet Comb., percent
Air Heater Air In, °F
Air Heater Air Out, °F
Boiler Gas Out, °F
Attemp. Steam Out, °F
Undergrate Air, °F
A.H. Gas Out, °F
I.D. Fan Gas In, "F
Feedwater Temp., °F
Wood Feedscrews Load, percent-,— 1/2/3 -
Air Heater Air Inlet Damper Percent Open
Tempering Air Damper Percent Open
Gas Burners In Service
Register Setting Percent Open ' / ^
/#//-/
Z-17-76
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Comments:
Mtric.
re
50 1
2 frf f**-
-------
OPERATING DATA
Location 10
Unit 1
Test No.
Date
Time
Steam Flow, Ib/hr * )O~*
.Steam Outlet Press., psig
Steam Outlet Temp. , °F
Burner Gas Press., psig
Furnace Draft, in. H.,0
Main Undergrate Air Press., in. H.,0
Primary Air Press. , in. H_0
A.M. Air Outlet Press., in. H.,0
A.H. Air Inlet Press., in. H.,0
F.D. Fan Discharge Press., in. H.,0
Low. Over fire Air Press., in. H.,0
Up. Over fire Air Press., in. H_O
I.D. Fan Inlet Draft, in. H,0
A.H. Gas Out, in. H_O
Boiler Outlet Draft, in. H.,0
Undergrate Air Flow, percent
Wood Steam Flow, percent
Windbox Air Flow, percent
Total Air Flow, percent
Gas Flow to Burners, SCFH
Boiler Outlet O,, percent
Boiler Outlet Comb., percent
Air Heater Air In, °F
Air Heater Air Out, °F
Boiler Gas Out,. °F
At temp. Steam Out, °F
Undergrate Air, 8F
A.H. Gas Out, °F
I.D. Fan Gas In, °F
Feedwater Temp., °F
Wood Feedscrews Load, .percent* 1/2/3
Air Heater Air Inlet Damper Percent Open
Tempering Air Damper Percent Open
Gas Burners In Service
Register Setting Percent Open •/ 2.
3/y
10//-2
f~/1-7€
l3'-/f
if*-t?r
#20
740
1.0 (fliti.FloVj
-,3
—
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7.6
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27
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ALSO
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502
Bo '/f AlFt
-------
OPERATING DATA
Location 10
Unit 1
Test No.
Date
Time
Steam Flow, Ib/hr * tO~*
Steam Outlet Press., psig
Steam Outlet Temp. , °F
Burner Gas Press. , psig
Furnace Draft, in. H,O
Main Undergrate Air Press., in. H.,0
Primary Air Press., in. H,0
A.H. Air Outlet Press., in. H,0
A.H. Air Inlet Press., in. H,0
F.D. Fan Discharge Press., in. H,0
Low. Over fire Air Press., in. H,0
Up. Overfire Air Press., in. H,0
I.D. Fan Inlet Draft, in. H,O
A.H. Gas Out, in.;H,O
Boiler Outlet Draft, in. H.,0
Undergrate Air Flow, percent
Hood Steam Flow, percent
Windbox Air Flow, percent
Total Air Flow, percent
Gas Flow to Burners, SCFH
Boiler Outlet 0^, percent
Boiler Outlet Comb., percent
Air Heater Air In, "F
Air Heater Air Out, °F
Boiler Gas Out, °F ".
Attemp. Steam Out, °F
Undergrate Air, 'f
A.H. Gaa Out, aF
I.D. Fan Gas In, °F
Feedwater Temp. , °F
Wood Feedscrews Load, pamontT 1/2/3
Air Heater Air Inlet Damper Percent Open
Tempering Air Damper Percent Open
Gas Burners In Service .
Register Setting Percent Open ^ '/'^~
10/1-3-
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211
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3-0 100
Commentsi
503
-------
OPERATING DATA
Location 10
Unit 1
Test No.
IO//-2.
I0//-2-
IO//-2-
Date
2-2.1-76
Time
13 "-
Steam Flow, Ib/hr * IP
~
200 -
Steam Outlet Press., psig
#70
Steam Outlet Temp., °F
7 &?-%/£>
710
72?
Burner Gas Press., psig
Furnace Draft, in. H.,0
* y
-.3
Main Undergrate Air Press., in. H.,0
Primary Air Press., in. H.,0
A.H. Air Outlet Press., in. H.,0
t.2-
(.2-
A.H. Air Inlet Press., in. H.,0
Z
7*7
7.C
F.D. Fan Discharge Press., in. H^O
X.I
Low.Overfire Air Press., in. H.,0
2-6
Up. Overfire Air Press., in. H.,0
27.5-
27
27
I.D. Fan Inlet Draft, in. H.,0
-2
-7.6
-7,2
A.H. Gas Out, in. H.,0
-f.v
-1.2-
-1.1
Boiler Outlet Draft, in. H.O
-3
'2.7
Undergrate Air Flow, ..percent
32
33
32*5'
Hood .Steam Flow, percent
5*0 -
£2-72-
Hindbox Air Flow, percent
2-tf
2?
Total Air Flow, percent
Gas Flow to Burners, SCFH
113000
g/ '000
Boiler Outlet O.,, percent
1-3
0 -
Boiler Outlet Comb., percent
Air Heater Air In, "F
105"
Air Heater Air Out. "F
5-70
Boiler Gas Out, °F
702-
717
Attemp. Steam Out, "F
672-
Undergrate Air, "F
A.H. Gas Out, °F.
I.D. Fan Gas In, °F
sir
Feedwater Temp., °F
21 /
Wood Feedscrews Load, percent, 1/2/3
7 \ .7 \7.
Air Heater Air Inlet Damper Percent Open
Tempering Air Damper Percent Open
Gas Burners In Service
-------
LOCATION IO/I
.FUEL GAS CHBOMATOGRAPHIC ANALYSIS
CHROMATOGRAPH
ANALYSIS; Mot $ GPM ©14.65 PSIA
CARBON o10x1DE 0.10
NITROGEN 0^88
METHANE 95*6H/-
ETHANE 2.04
PROPANE 0*.70 0.195 ,
ISO-BUTANE 0.15 0.049
N-BUTANE o.2l O.o6b
ISO-PENTANE 0.06 0.022
N-PENTANE 0.06 0.022
HEXANES PLUS p. |6 . 0.968
IOO.OO 0.419
SPECIFIC GRAVITY @ 60° F. (AIR == l) 0.5891
B.T.U./CU. FT. @ 14.696 PSIA AND 6o°F.:
DRY BASIS 1044
WET BASIS ........ .1026
505
-------
Test 10/1-2
LOCATION 10
Unit 1
FUEL ANALYSIS'
August 19, 1976
5:15 p.m.
Basis
Proximate analysis:
Moisture, %
Volatile matter, %
Ash, %
Fixed carbon, %
Ultimate analysis:
Moisture, %
Carbon, %
Hydrogen, 7o
Nitrogen, 7,
Sulfur, 70
Ash, 7o
Oxygen, % (by difference)
Heat of Combustion:
Gross BTU/lb
Net BTU/lb
As received
50.69
36.54
2.27
10.50
Dry
74.10
4.60
78.70
50.69
25.32
2.73
0.15
0.05
2.27
18.79
4362
4108
51.34
5.54
0.31
0.11
4.60
38.10
8845
8331
506
-------
PAKTICUIATE EHISSION CALCULATIONS
• /*
Test No. /0/t'/ Date.
Unit Mo. /
Pitot Factor, Fs
location
Fuel #6. f OtfpocS Load
IS #
Barometric Pressure, P. .
in. Hg
Tot. Liquid Collected,
ml Total Particulate, Mn /926~3 m gn
Velocity Head, AP__1£ssl_iwg Stack Temp. , T8_jZ£^__»R Stack Area,
'ft
Sample Volume, Va
ft
Stack Press., Psg - "
* H/13.6)
n.d.
4. Concentration a. C • 0.0154 Mn/Vm
•td
b. C - 2.205 x 10"6 Mn/V«n>td
C. C - Eq. 4b x 16.018 x 103
5. Aba. Stack Press. Ps • P.^ x 13.6 + Psg
6. Stack Gas Speed Vs • 174 Fs /APTs J~' x
7. Stack Gas Flow a. Qsw • Eq. 6 x As x fjp x ~-
Kate « 70°F • 40/
b. Qsd • Eq. 7a x (1. - Eq. 3)
a. Material Flow
9. JCO. factor
10. Emission
11. % Isokinetic
Ms - Bq. 7b x Eq. 4b x 60
XOjf • 2090/(20.9 - X02%)
a. E - Eq. 4b x Fe x Bq. 9
b. E • Eq. 4c x Fn x Eq. 9 x 1000
14077 x Ts(Vm + Vw )
I . 2 _S
6 x Vs x Ps x Dn
Fe SC Feet/104 Btu
Fm 'SC Meters/104 joules
Oil
92.2
0.002475
Gas
87.4
0.002346
Coal
98.2
0. 002636
in.
SCF
~*
400,
J0.f
-------
PARTICIPATE EMISSION CALCULATIONS
froc/.f. rre/t..&-
Test Bo. /0//-/ Date g-/g-7£ Location,/
-—•
Unit No. / Fuel /#<£. / U?*e>c/ Load
Pi tot Factor, Fs
Barometric Pressure, P
bar-
mi Total Particulate, H
in. Hg
9 m gm
Tot. Liquid Collected, V
Velocity Head, AP . ffj>" iwg Stack Temp., Ts__£^£__*R Stack Area,
Sample Volume, Vm 62.£Zf*? Stack Press., Psg -£ 7 iwq Excess 02, K> *_
Orifice Press. Diff., H -S/6 iwg Stack Gas Sp. Gravity, Gs_
Sample Time, 6 S20 min Nozzle Diameter, Dn . «5"
1. Sample Gas Volume Vmstd - 0.0334 Vm(P + H/13.6)
2. Hater Vapor ^std " °'0474 vic
3. Moisture Content Bwo » Eq. 2/(Eq. 1 -f Eq. 2)
n.d. «v/.
4. Concentration a. C « 0.0154 Hn/Vm
Btd
b. C - 2.205 x 10~6 Mn/V»
C. C - Eq. 4b x 16.018 x 10
5. Abs. Stack Press. Ps • P x 13.6 + Psg
8td
3
6. Stack Gas Speed Vs • 174 Fs /APTs /r^
1.00
Gs
7. Stack Gas Flow a. Qsw « Eq. 6 x As x —— x rlr-
Rate 0 70°F Ts 4O7
b. Qsd - Eq. 7a x (1. - Eq. 3)
ft. Material Flow Ms - Eq. 7b x Eq. 4b x 60
»2f - 2090/(20.9 - X>a%)
10. Emission a. E • Eq. 4b'x Fe x Eq. 9
9. X0_ factor
11. » Xsokinetic
b. E - Eq. 4c x Fa x Eq. 9 x 1000
14077 X
6 x Vs x Ps x Dn
Fe SC Feet/104 Btu
Fn «SC Meters/104 joules
Oil
92.2
0.002475
Gas
87.4
0.002346
Coal
98.2
0.002636
in.
SCF
N.D.
grains/DSCF
X
, grams/DSCM
, in. w abs.
. ft/min
WSCF/min
.DSCF/min
. Ib/hr
Ib/MMBtu
ng/joule
Data Sheet 6002-4
508
-------
PARTICUIATE EMISSION CALCULATIONS
Test No._/fe^_£__ Pate £-r '
Nozzle Diameter, Dn ~37tT in.
n.d.
1. Sample Gas Volume Vm - 0.0334 Vm(P. + H/13.6)
Bta oar
Vw . . - 0.0474 V.
std Ic
2. Hater Vapor
3. Moisture Content Bwo •* Eq. 2/(Eq. 1 + Eq. 2)
4. Concentration a. C - 0.0154 Mn/Vm ...
sta
b. C - 2.205 x lo"6 Mn/Vm
C. C • Eq. 4b x 16.018 X 10
5. Abs. Stack Press. Ps - P x 13.6 + Psg
etd
3
6. Stack Gas Speed Vs - 174 Fs /APIs Jj~* ^f/^
7. Stack Gas Flow a. Qsw - Eq. 6 x As x ^22 x E£_
Kate 6 70°F Ts 407
b. Qsd » Eq. 7a x (1. - Eq. 3)
& Material Flow Ms - Eq. 7b x Eq. 4b x 60
JtOjf - 2090/(20.9 - Jff>2%)
10. Emission • a. B • Eq. 4b x Fe x Eq. 9
b. E - Eq. 4c x Fm x Eq. 9 x 1000
9. XO, factor
11. % Isokinetic
14077 X T8(Vm * Vw)
6 x Ve ic PS x Dn
Fe SC Feet/104 Btu
Fm SC Meters/104 joules
Oil
92.2
0.002475
Gas
87.4
0.002346
Coal
98.2
0. 002636
//
-------
Test HO.
Unit No.
PARTICULATE EMISSION CALCULATIONS
'/ f? • 74 Location
/
Fuel MA f /f
-------
Teat Ho.
Box No. *
Test Description
PAKTICUIATE CALCULATION SHEET
Date J-/f-7f location.
' Sample Probe Position
10
Tut Craw
Dry 6*a Neter Vol. (ft')
Final fY/Y,2f
Initial (3rt.7£
fetal ei.fJ.
Impinger Water Vol (ml)
1 2
Final ** y 70
Initial /oo /tfo
A Vol A97 -30
Beaker Ho. / •* 3
IT,. . 9~n—?t _
Neighed * '' 7*
Tare 1 too. 01 33
Wt. 2/00,0T3V
3
4
S
6
jws ,'oo. of ay
Bottle Ko. / * -2.
Iqpinger
Content (Water)
Rinae (ml) 72 5"
Date Sighed
or 2SO Bake *~*O'ff
Final 1 100.1/3*
Wt. 350 1IOO.II3F
3
4
5
6
Avfl/oA//5r
Raaidue wt
Final KQ-ftx*.02Ol
Date Weighed
or 650 Bake
Final 1
Wt. 650 2
3
4
5
6
Avg
Reeidue Wt
Final 650-Tare
IOI.S3VO
101.63. V3
101. (2*3.
S
Probe
(Acetone)
S-7S-
lt>3..3S$3.
10 3.. 13-32.
102.33-93.
.7210
lei. 1t(3
Iff/, 116?
let, 186V
1
Probe
(Water)
HZO
»OI.11(7
101. lift
I0I.11S7
.010$
~"\
J
^VfllMI^
3 6. Gel Total
•«• rf'rV. 7 lega. 7
&• jtee.7 ?to.7
&•
V
?y.7«5"
4.32.0
Filter
No.
r
.9V26
.1i*V
.SH3.7
t-ft-7£
*1<3*
.1(37
.1(3 (
,H3f
.12.01
Blank
No.
(
.9077
.9079
.9078
*-rt'7£
.307S
.to7t
.S07S
•»• •
Comnentai
Data Sheet 6002-3
5 1 1
-------
PARTXCULATE CALCULATION SHEET
Test tto. I0//-3- Date 2-2 J-7* location
Box Mo. Sample Probe Position
Vest Description
Test Crew
to
Dry Gas Meter Vol. (
Final HlO.tf
Initial /yy/.FV
Total fl.tS.
Beaker No. 5~
D*** F-/7-7X--
Weighed * ' ' '6
Tare 1
f ff
~^clp»e-*'
^<*eet3r»0^
Water Vc
3
/ <
^- t
1
3
^
^
1 (ml)
S. Gel 1
f 72. 7 It
rrf. 8 i
It. f j.
Filter
No.
£
ff— /7- ff
.8077
.9073
.W7f
S-2S-7{
l.21*i
1.2196
1.2191
t,21*7
.itt>i
^^tal
?}. 7 ,
ff,1
*7.1
Blank
No.
7
9 - 17- 7(
,Si61
.817*
.W70
V-2S--7t
.81f1 -
rgVf1 .
,iiff
-^-
Comment*s
Data Sheet 6002-3
5 1 2
-------
PLANT
METHCJt) 5 COMTKOL CONSOLE READINGS
LOCATJON fo"
OPERATOR
DATE g-iSf-7,
RUN NO. .
SAMPLE BOL ..
METER BOX NO
4ETER H
lo//-/
OX NO.
2 FACTOR"? TgF
AMBIENT TEMPERATURE
BAROMETRIC PRESSURE
ASSUMED MOISTURE, %
HEATER BOX SETTING ~
PROBE LENGTH, IN.
NOZZLE DIAMETER, IN.
PROBE HEATER SETTING
3~
SCHEMATIC OF STACK CROSS SECTION
Traverse
Point
limber
TOTAL
WERAGE.
Sampling
Time
(e)Mifrr
CtOe.K
rtfie
1103.' iO .
lll7:io
1/32 :fo
IIW/0
)20^''iO
I3.l7".f0
i3.9z:fo
I2f7:f0
1102.' 10
13.0 **£*,,
static
Pressure
(P8),
^— ••• —
jiii v iiy i
i»J
r-^,-7
\
'
Stack
Tempera-
ture
I3£*.oo
177*. 0o
uti.eo
ISt/,?*
1311.00
If Of .00
/y/y.2*
gz.fzj*.*
Gas Sample
Temperature at
Dry Gas Meter
Inlet
•P
ir
I*
100
wy
IP?
//£>
US'
12-0
120
AVG.
AVG.
Sample
Box
remprta-
ture
•F
//^
}?0
3^0
13-0
>**
320
?3f
3 i0
33?
ftVP-
Temperature
of Gas
Leaving
Condenser on
^ast Impinger
•F
7^
/«
70
70
&
f0
fo
S0
£S~
01
CJ
-------
PLANT
LOCATION"
OPERATOR"
DATE
IV/tUCH) 5 OU3XRUL
HEADINGS
10
g-IS~
RUN NO.
SAMPLE BOX*
METER BOX NO.
4ETER H--. '
- FACTOR 8' ,
AMBIENT TEMPERATURE
BAROMETRIC PRESSURE *
ASSUMED MOISTURE, %
HEATER BOX SETTING
PROBE LENGTH, IN.
NOZZLE DIAMETER, Wr
PROBE HEATER SETTING
SCHEMATIC OP STACK CROSS SECTION
Iff FACT OK
Point
TOTAL
,,mf,,^T-
Sampling
Time
CLOC.K.
113?
Ifif
HT0
/yrr
lift
- - If '
• -.: -
. ,.: •' . >'-
-.
Static
Pressure
<*£
-r.0
>
Stack .
Tempera-i
ture
if
it*
it*
if*
-
Velocity
Head
Pressure
)ifferen-
tial ACTOE
Orifice
Meter
(AH),
In. H2O
.00$-
.006
.00C
.0°G
s Gas
Sample
Volume
*V ft3
\
HI 6. 00
HI 7. oo
ilH.oo
If/f.ff
Gas Sample
Femperature at
>ry Gas Meter
Inlet
(Tmin.)
°p
Outlet
op
ir
1?
1?
11
t
AVG.
..... . -
Sample .
Box
Temprta-
ture
•F
-
AVR.
Temperature
of Gas .
Leaving
Condenser on
iast Impinger
•F
70
70
70
70
•".. -' • • •
en
-------
10
PLANT
LOCATION"
OPERATOR"
DATE a
RUN NO.
SAMPLE BOX NO.
METER BOX NO.
4ETER H
2 FACTORT
RSADXMGS
I0//-2.
AMBIENT TEMPERATURE
BAROMETRIC PRESSURE *
ASSUMED MOISTURE, % '
BEATER BOX SETTING *
PROBE LENGTH, IN.
NOZZLE DIAMETER, IN."
PROBE HEATER SETTING"
y/.
SCHEMATIC OF STACK CROSS SECTION
Traversa
Point
Motor
TOTAL
\trrn?/"f
Sampling
Time
(e)Mtnr
c*»e*
r/f£
II to
iirr
12-10
I2-3-*
A2V*
I2.ST
I3te>
13**
I3io
I2t>^
Static
Pressure
(P8) ,
In. Itg^HjO
-1.3
^
i
Stack
Tempera-
ture
(Tg) »F
y/
•P
/e>r
1*5-
110
It*
111
12-0
12.0
12-0
12-0
AVG.
Sample
BOX
Pemprta-
ture
•P
3/0
3FO
120
3*0
3?0
3*0
310
3/0
3^0
&VR-
Temperature
of Gas
Leaving
Condenser on
iiast Impinger
•P
/^
&••
*f
S*~
£3-
f*
f*
fT
63
en
01
-------
PLANT _
LOCATfoTT
OPERATOR"
DATE s
METHOD S CCMTHUk CONSOLE READINGS
10
RUN NO. /Q/l-
SAMPLE BOX NO.
METER BOX NO. *
4ETER H ~
3 FACTOR"?
AMBIENT TEMPERATURE
BAROMETRIC PRESSURE "
ASSUMED MOISTURE, % "
HEATER BOX SETTING "
PROBE LENGTH, IN. "
NOZZLE DIAMETER, -H»r~
PROBE HEATER SETTING"
Mj_
SCHEMATIC OP STACK CROSS SECTION
Traverse
Point
timber
TOTAL
"* t f r» T> * r»*~
Sampling
Time
(e)Miiw-
Ci»e-K
r/fif
HHO
in?
H5~0
ii?s~
)5~4H*t».
Static
Pressure
(P8),
in. tier*.
»**
-1.H
V
Stack
Tempera-
ture
itr
Velocity
Head
(P8)
Pressure
Differen-
tial Acros
Orifice
Meter
(AH),
In. H2O
,^J
.03
.*y
s Gas
Sample
Volume
Hfrf/t ne**M
•P
HO
/£>r
It*
AVG.
Sample
Box
Pemprta-
ture
°F
AVR.
Temperature
of Gas
Leaving
Condenser on
[•ast Impinger
•F
zr
en
a>
-------
Test No.
CASCADE IMPACTOR DATA SHEET
TEST RUN NO.
IMPACTOR NO.
"LOCATION
DATE
CYCLONE NO.
OPERATOR
SAMPLE POINT LOCATION
0? A.tf. .
0V fT
SUBSTRATE COATING '_ M0A/£-
FUEL
TEST LOAD
IMPACTOR ORIENTATION
FLUE STATIC PRESSURE ~& 0
V
FLOW THRU IMPACTOR
_inH20, VELOCITY
NOZZLE DIA.
GAS METER END
CF
GAS METER START
GAS VOLUME */
nun IMPACTOR PRESSURE DROP /#• / Ajx^END TIME
START TIME _
DURATION
CF
FLOW RATE
AMBIENT TEMPERATURE
FLUE GAS MOLECULAR NT.
_'F PRESSURE ^ f > 7 IN Hg. HUMIDITY
, TEMP.
.klb/hr
CFM
CFM
F, DENSITY
g/cc,VISCOSITY
POISE
Foil + Sample, g
Unused Foil, g
Sample, g
Correction
for Blank, g
Final Sample, g
Stage Number
1
5.67i3.
Uftt
.01*3
2
3.^5-ya
3L1W
,
-------
Test No.
TEST RUN NO.
IMPACTOR NO.
CASCADE IMPACTOR DATA SHEET
"LOCATION
DATE
CYCLONE NO.
OPERATOR
SAMPLE POINT LOCATION
SUBSTRATE COATING
,#. g£f0#£
IMPACTOR ORIENTATION
FLUE STATIC PRESSURE
NOZZLE DIA. 'i
FUEL M 6.+MAK TEST LOAD
FLOW THRU IMPACTOR
CFM
_inH20,VELOCITY_
GAS METER END
GAS METER START I*(W.5*OCE
GAS VOLUME 2
AMBIENT TEMPERATURE
mm IMPACTOR PRESSURE DROP // END TIME
CF START TIME / J /
DURATION _ '_
FLOW RATE
,13
CFM
FLUE GAS MOLECULAR WT.
_*F PRESSURE 21,%$" IN Hg. HUMIDITY
•
, TEMP.
F, DENSITY
g/cc,VISCOSITY
POISE
Foil + Sample, g
Unused Foil, g
Sample, g
Correction
for Blank, g
Final Sample, g
Stage Number •
1
^22f
v.mjz
.0036
2
3.ftfl
3.M31
;00I2
3
W/07
W7W
.000*1
4
3. (701
^.6 70S
.0006
5
wr?
1.I7F2
. ooo?
Stage
Blank
FILTER NO.
Sample Blank
FILTER + SAMPLE, g
FILTER TARE, g
SAMPLE, g
CORRECTION FOR
_ BLANK, g
_ FINAL SAMPLE, g
1.2007
1.2027
-.002.0
FULL CONTAINER, g
EMPTY CONTAINER, g
CYCLONE CATCH, g
1 8
60-20
-------
TABLE 1.
Symbol
Pressure drop across impactor
during test "Hg"
Static pressure at inlet to
impactor, atm.
Density of aerosol particle, grams/cc
Density of gas at inlet sampling
conditions, grams/cc
Molecular weight of sample gas
Molecular weight of calibration gas
Temperature of gas at sampling
conditions, °K
Temperature of gas at calibration
conditions, °K
Static pressure under calibration
conditions, atm.
Gas viscosity at sampling conditions,
poises
Stage jet diameter, cm
Sample quantity collected on each cup.
MW
y
D
2.
0.177?
O.131*
0.01f6
0.0731
3.6
1.2.
4
R5
0,6
Dimension conversion constant
5 1 9
-------
TABLE 2.
Effective pressure drop, "Kg"
Inlet flow to impactor, cc/ 'second
Pressure out of stages, atm.
Density of gas out of the various
stages, grams/cc
Characteristic diameter, microns
Criteria for validity of equation
Mean free path
Symbol Value
APE 1. 72-
F Zf, /5~
P- 0..11
^2 ~- — si '"'
Pr3 0,11
P? *,1*
p_5 0- 1ST
°6
2 -, « -«/
?„ 7,2-t/o i
P? 7.3 'If"
,'.* 7.1"°-*
P? H't*-*
"f-
o6 3.17
o^2 2-31
o^3 /. n
D^4 ..-0.9.2..
P 5 <~
18 ^XIO'4
6 V i
Average molecular Velocity
. 75*0
Continued
520
-------
TABLE 2 (Continued)
Symbol Value , cfCLONE.
* on a cup of the total sample collected
Stage 2
3 Y3 _LLJ-
« Y4 >3'* ,
5 Y5 ?.* I
6 Y6 7.J 1.0?
Filter Y7 <9 O
Total 100.00*
•Any discrepancy due to rounding off should be buried
in the largest Y cumulative % smaller than D
52 1
I2 17.0 /. 73
I^ If, 2. 2-31
h
Z6
-------
PLUME OPACITY OBSERVATION RECORD
Test Run Ko.
LOCATION NO.
3WNER
DATE
OBSERVER
BOILER NO.
CAPACITY
AUG 1 8 1976
VFUEL TYPE ggw/^y/^EURNER TYPE
POINT OF EMISSION
POINT OF OBSERVATION
•/
klb/hr
TEST •
No.
I"
1
Tine
anv/pnr
frtf
ir. 17
//: /f
fl-if
If: 13
If-lf
if-i)
II i 1
it-.tr
»'
-------
»roj«cti_
Oat* i
Locationi_
Onlt<_
Tests.
Fuel i
VELOCITY TRAVERSE
Test DescriptionI
Stack Cross Section
Personneli
Barometric Press, (in. Bq)i
Absolute Static Press, in Stack (in. 89) i_
Pitot Tub* Coefficient!
- 65.48
1/2
Tiae
Traverse Point
Port Depth
1
I
tAtJO
[
2.
3
i
f
f
7
Velocity
Bead
(in. B20)
ta
,07
.sf
.0?
.01
.0?
.0?
.of
Gas Tenp.
CF)
Gas Temp.
CR)
TS
Molecular
trt.
ns
Velocity
(ft/sert
vs
02
Cone.
(% Dry)
1
6002-11
523
-------
»rojecti_
Date i
location!
VELOCITY TRAVERSE
Tut Description t
Stack Cross Section
to/I-
Personnel!
Dniti_
»sstt
Poeli
Barometric Press, (in. Bg)s
Absolute Static Press, in Stack (in. Bg)t_
Pitot Tube Coefficient!
(P.)
V. - 85.48
TilH
Traverse Point
Port Depth
BMD
\
2.
3
.
(•r>
Gas teap.
CR)
TS
Molecular
Wt.
MS
Velocity
(ft/sec*
vs
°2
Cone.
(% Dry)
6002-13
524
-------
BLACK LIQUOR RECOVERY BOILER
Location No
. \Q
Unit. No.
Unit. Description
~Re.CO Vfe
Installation Date
Heater Rating
Burner Description OQUrP>O£>TtO*>i
. O
Test Fuel Combinations
Fuel Temp, at Bvirner (°F)
J
Primary Air Temp. (°F) 422. >< (>QQ OF" )
Comments:
525
-------
Test No._
Unit Ho.
•"3
Unit Type
MOBILE LABORATORY DATA
Date "*o -76.' Location .
fuelf/cl:. iftji4. Capacity
fir. Burner Type
Test Ho.
Engr.X
1. Test Ho.
2. Date
3. Time
4. Load '
5. Process Rate •
6. Flue Diam. or Size, ft
7. Probe Position
8. Oxygen (%)
9. NOx (hot) read/3% 02 (ppm)
10. HO (hot) read/3% 02 (ppm)
11. NOa (hot) read/3% 02 (ppm)
12. NO (cold) read/3% 02 (ppm)
13. Carbon Dioxide (%)
14. Carbon Monoxide (ppm) uncor/cor
15. Hydrocarbon (ppm) uncor/cor
16. Sulfur Dioxide (ppm) uncor/cor
17. Smoke Spot (Bacharach)
18. AtmoB. Temp. (•F/*C)
19. Dew Point Temp. (*F/*C)
20. Atmos. Pressure (in. Ha)
21. Relative Humidity (%)
22.
23.
24.
25.
26.
27.
28.
29.
30.
ie>/2-l
f'2g'7f
/f'ff
)7g
3f1f*22't"
~j'f';*
tff
/
/
12-
ff.
mo
^
f
/*
'
7
2^
^/
2~
32.
i
20DO
i&j-
17*1
**£?•
//"
77
21.11
70
•
Data Sheet 6002-2
526
-------
tot
Test No.
Unit No.
Unit Type <•
'7. a -C MOBILE LABORATORY DATA
*• "v *V
"If. Date f'3l*7£ Location 16
3- *»\Blck.tin*. capacity 2.1 f * l**'Sf#
'£ fief* \ffry fir. Burner Typa
T««fc No. ~ *» .
Bngr. 9ilfA//A/G
1. Test No.
2. Date
3. Time
4. Load
5. "Process Rate
6. Flue Dian. or Size, ft
7. Probe Position
8. Oxygen '(%)
9. NOx (hot) read/3% 02 (ppm)
10. NO (hot) read/3% 02 (ppm)
11. N09 (hot) read/3% 02 (ppm)
12. NO (cold) read/3% 02 (ppm)
13. Carbon Dioxide (%)
14. Carbon Monoxide (ppm) uncor/cor
IS. Hydrocarbon (ppn) uncor/cor
16. Sulfur Dioxide (ppm) uncor/cor
17. Smoke Spot (Bacharach)
18. A tubs. Temp. (°F/*C)
19. Dew Point Temp. (sF/eC)
20. Atmos. Pressure (in. Hg)
21. Relative Humidity (%)
22.
23.
24.
25.
26.
27.
28.
29.
30.
10/2'H
3-3f-?f
i-
>
l{2?
Jf0
y
2i
22.
\
JZ
•f
>
i/a
tti
77
7f
2l.t*
If
lt>/2'&
g-3t-?£
I3S2.
'15"
i
f,,
27
27
/
^y
a
nttts
jeto
It 00
2.00
• «•••••
7
3(
3*
(
?f
f
—
fft-
221
tr
78
21.1 1
71
/'/*-£
X-3t-7f
1(21
I7f
I
3,
22
2f>
3. •
32
/f
%ooo
"iriff
ioo
^^»
r
23
2.f
2.
33
,\
— •
'*?*>
Ill
••i
f7
7g
3-1 '12
41
.
•
8heftt_6002,2-
xs
52;
-------
MOBILE LABORATORY DATA
10/1 -7, -
Test Ho. -°i
Test No.
Unit No.
Unit Type <
y ~j
~°l - Date y~l-7( Location /* Engr. fvf*lifl&
2- tve\£/ck. (• Itfu. Capacity ^/5" * 1° rfn
'£ Kftetfe'i' gt-f. Burner Type
1. Test No.
2. Date
3. Time
4. Load
5. Process Rate
6. Flue Diam. or Size, ft
7. Probe Position
8. Oxygen (%)
9. NOx (hot) read/3% 02 (ppm)
10. NO (hot) read/3% 02 (Ppm)
11. NO? (hot) read/3% 02 (ppm)
12. NO (cold) read/3% 02 (ppm)
13. Carbon Dioxide (%)
14. Carbon Monoxide (ppm) uncor/cor
15. Hydrocarbon (ppm) uncor/cor
16. Sulfur Dioxide (ppm) uncor/cor
17. Smoke Spot (Bacharach)
18. Atmos. Temp. (°F/°C)
19. Dew Point Temp. (°F/eC)
20. Atmos. Pressure (in. Hg)
21. Relative Humidity (%)
22.
23.
24.
25.
26.
27.
28.
29.
30.
10/2-1
1- /- ?(
e?t>0
/85~
2.3
13
12.
\
2\
13.
Excess
ieoo
220
• ••
IS
12-
1
2}
3
•>
106t
221
?0
77
21.83
ft
10/2 -8
f-t~7(
/0:}C>
200
3.7
17
1?
0
2-f
ff.
>2CX.
ifao-
22^
I!
ft
0
2-S
0
<0
Jf'/S
22?
••«.
85
77
2-1.S1
71
10/2 "1
?-/'/?
l/'/f
)ff
#
ff
If
1
21
11.
>2C.
3ff(>
21 e>
/
20
/
-------
, _ . •
IO/T.-/Orll C
Test No. **/?- Date ^-
MOBILE LABORATORY DATA
Location _ IP
Test No.
-/Z
Engr. WOOD
Unit No.
Fuelfl*. //y. Capacity
Unit Type///:
Burner Type LigueA. for fief
1. Test No.
2. Date
3. Time
4. Load
5. Process Rate
6. Flue Diam. or Size, ft
7. Probe Position
8. Oxygen (%)
9. NOx (hot) read/3% Oj (ppm)
10. NO (hot) read/3% 02 (ppm)
11. NO? (hot) read/3% 02 (ppm)
12. NO (cold) read/3% O2 (ppm)
13. Carbon Dioxide (%)
14. Carbon Monoxide (ppm) uncor/cor
15. Hydrocarbon (ppm) uncor/cor
16. Sulfur Dioxide (ppm) uncor/cor
17. Smoke Spot (Bacharach)
18. Atmos. Temp. ("F/'O
19. Dew Point Temp. (0F/°C)
20. Atmos. Pressure (in. Hg)
21. Relative Humidity (%)
22.
23.
24.
25.
26.
27.
ZB.
29.
30.
10/J-IO
f-/r~7s
112.0
^
23
*•(
2.
35
f f *
17200
I5M
Ifo
"•.-•
7
2f
25
3.
?{
0
30W
HSS
50$
ft
7S
2/2->\
1-l(-7t
0820
i.o
2F
2S~
0
31
J2.
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529
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Test Ho
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MOBILE LABORATORY DATA
- 21 -76 Location / O
Test NoJwZ--
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Capacity,
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12. NO (cold) road/3% 02 (ppm)
13. Carbon Dioxide (%)
L4. Carbon Monoxide (ppm) uncor/cor
15. Hydrocarbon (ppm) uncor/cor
16. Sulfur Dioxide (ppm) uncor/cor
17. Smoke Spot (Bacharach)
18. Atmos. Temp. (°F/^O
19. Dew Point Temp. C'F/'X)
20. Atmos. Pressure (in. Hg)
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22.
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530
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MOBILE LABORATORY DATA
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53 1
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Test No.«>/2->4
Unit No. 2.
MOBILE LABORATORY DATA
Date 3-I.V76 Location tO
Test No
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13. Carbon Dioxide (%)
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15. Hydrocarbon (ppm) uncor/cor
16. Sulfur Dioxide (ppm) uncor/cor
17. Smoke Spot (Bacharach)
18. Atmos. Temp. (°P/\;)
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532
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Test Ho.
Unit Mo.
MOBILE LABORATORY DATA
Location JO
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Capacity.
Unit Type fettaJflgy I&L<, LT&. BOlL. Burner Type
1. Test No.
2. Date
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11. NO? (hot) read/3% 02 (ppm)
12. NO (cold) read/3% 02 (ppm)
13. Carbon Dioxide (%)
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IS. Hydrocarbon (ppm) uncor/cor
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Test No/P/2^ 15 Date?-2^-7(6 Location lQ
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Data Sheet 6002-2
534
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Test ttoJ '..•"_'
Onit No. ^
MOBILE LABORATORY DATA
location /D
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Unit Type %£(&>£&*/&£., Z6XZ ,
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10. NO (hot) read/3% 02 (ppm)
11. NOa (hot) read/3% 02 (ppm)
12. NO (cold) read/3% 02 (ppm)
13. Carbon Dioxide (%)
14. Carbon Monoxide (ppm) uncor/cor
15. Hydrocarbon (ppm) uncor/cor
16. Sulfur Dioxide (ppm) uncor/cor
17. Smoke Spot (Bacharach)
18. A tecs. Temp. (°F/»«J
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Data Sheet 6002-2
535
-------
MOBXLB LABORATORY DATA
VQ.I°/Z~I6 Ovt»t?'tt'l6 location lO
Unit Mo. 2- pueiSl^.l^g. capacity
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unit TypeEggQv)eg//ft.g-
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10. NO (hot) read/3% 02 (ppm)
11. NC5 (hot) read/3% 02 (ppm)
12. NO (cold) read/3% 02 (ppm)
13. Carbon Dioxide (%)
14. Carbon Monoxide (ppm) uncor/cor
15. Hydrocarbon (ppm) uncor/cor
16. Sulfur Dioxide (ppm) uncor/cor
17. Smoke Spot (Bacharach)
18. AtHDS. Temp. (*F/>C)
19. Dew Point Temp. (*F/»C)
20. Atmos. Pressure (in. Bg)
21. Relative Humidity (%)
22.
23.
24.
25.
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Data Sheet 6002-2
536
-------
MOBILE LABORATORY DATA
location I
Test'No.'
Unit No.
Unit
Capacity,
6o/l. Burner Type_
1. Test No.
2. Date
3. Time
4. load
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10. HO (hot) read/3% 02 (ppm)
11. N05 (hot) read/3% 02 (ppm)
12. NO (cold; read/3% 02 (ppm)
13. Carbon Dioxide (%)
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15. Hydrocarbon (ppm) uncor/cor
16. Sulfur Dioxide (ppm) uncor/cor
17. SmoXe Spot (Bacharach)
18. Atmos. Temp. (°F/\;)
19. Dew Point Temp. (eF/*C)
20. Atmos. Pressure (in. Hg)
21. Relative Humidity (%)
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24.
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Data Sheet 6002-2
537
-------
OPERATING DATA
Location 10
Unit 2
Test No.
Date
Tine
Steam Flow, Ib/hr
Steam Press., psig
Final Steam Temp. Before Attemp., °F
Final Steam Temp. After Attemp., °F
Burner Gas Press., psig
Black Liquor Solids, percent
Main Dissolving Tank Density
Percent 0, /Percent Combustibles
Total Air Flow, percent
Primary Air Flow, percent
Black Liquor Flow to Burners, GPM
Secondary Air Flow Damper pos. % open
Gas Flow to Recov. Boiler, SCFH
Black Liquor to Burner pressure, psig
Black Liquor to Burner temp. , °F
F.W. Temp., "F (typical)
Steam A.H. Air In, °F
Steam A.H. Air Out, °F
Boiler Gas Out, °F
L.H. Cascade Evap. Gas Out, "F/R.H.
East Econ. Gas Temp. , 'F/Hest Econ.
L.H. Precip. Gas Out/R.H. Precip., °F
Economizer Hater Outlet, °F
I.D. Fan Inlet Draft, in, H.,0
L.H./R.H. Precip. Out Draft, in. H.,0
Economizer Out Draft, in. H,0
Economizer In Draft, in. H.,0
Boiler Inlet Draft, in. H»0
Furnace Draft, in. H.,0
Secondary Air Pressure, in. H.O
Primary Air Pressure, in. H.,0
F.D. Fan Disch. Pressure, in. HnO
L.H./R.H. /New Case. Evap. Motor load, %
Black Liquor Burner In Service
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538
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OPERATING DATA
Location 10
Unit 2
Test No.
10/2-5
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Date
-; -76*
Time
0905
Steam Flow, Ib/hr
Steam Press., psig
Final Steam Temp. Before Attemp., *F
Final Steam Temp. After Attemp., °F
Burner Gas Press., psig
o
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7.5
Black Liquor Solids, percent
65
Main Dissolving Tank Density
Percent O,/Percent Combustibles
3,7
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L.H./R.H./New Case. Evap. Motor Load, %
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Black Liquor Burner In Service
Comments:
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-------
OPERATING DATA
Location 10
Unit 2
Test No.
Date
Time
Steam Plow, Ib/hr
Steam Press., psig
Final Steam Temp. Before Attemp. , °F
Final Steam Temp. After Attemp. , °F
Burner Gas Press. , psig
Black Liquor Solids, percent
Main Dissolving Tank Density
Percent O,/Percent Combustibles
Total Air Flow, percent
Primary Air Flow, percent
Black Liquor Flow to Burners, GPM
Secondary Air Flow Damper pos. % open
Gas Flow to Recov. Boiler, SCFH
Black Liquor to Burner pressure, psig
Black Liquor to Burner temp. , °F
F.W. Temp., °F (typical)
Steam A.H. Air In, °F
Steam A.H. Air Out, °F
Boiler Gas Out, °F
L.H. Cascade Evap. Gas Out, "F/R.H.
East Econ. Gas Temp., "F/West Econ.
L.H. Precip. Gas Out/R.H. Precip. , °F
Economizer Water Outlet, "F
I.D. Fan Inlet Draft, in. H.,0
L.H./R.H. Precip. Out Draft, in. H_O
Economizer Out Draft, in. H.,0
Economizer In Draft, in. H^O
Boiler Inlet Draft, in. H,0
Furnace Draft, in. H_O
Secondary Air Pressure, in. H.,0
Primary Air Pressure, in. H.O
F.D. Fan Disch. Pressure, in. H,O
L.H./R.H. /New Case. Evap. Motor Load, %
Black Liquor Burner In Service
10/2.- 3
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OPERATING DATA
Location 10
Unit 2
Test No.
Date
Time
Steam Flow, Ib/hr
Steam Press., psig
Final Steam Temp. Before Attemp., "f
Final Steam Temp. After Attemp. , °F
Burner Gas Press. , psig
Black Liquor Solids, percent
Main Dissolving Tank Density
Percent 0,/Percent Combustibles '
Total Air Flow, percent
Primary Air Flow, percent
Black Liquor Flow to Burners, GPM
Secondary Air Flow Damper pos. % open
Gas Flow to Recov. Boiler, SCFH
Black Liquor to Burner pressure, psig
Black Liquor to Burner temp. , °F
F.W. Temp., °F (typical)
Steam A.H. Air In, "F
Steam A.H. Air Out, °F
Boiler Gas Out, °F
L.H. Cascade Evap. Gas Out, °F/R.H.
East Econ. Gas Temp. , °F/West Econ.
L.H. Precip. Gas Out/R.H. Precip., °F
Economizer Water Outlet, "F
I.D. Fan Inlet Draft, in. H.,0
L.H./R.H. Precip. Out Draft, in. H,O
Economizer Out Draft, in. H.,0
Economizer In Draft, in. HnO
Boiler Inlet Draft, in. H.,0
Furnace Draft, in. H.,0
Secondary Air Pressure, in. H.O
Primary Air Pressure, in. H_0
F.D. Fan Disch. Pressure, in. H.,0
L.H./R.H. /New Case. Evap. Motor Load, %
Black Liquor Burner In Service
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54 1
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OPERATING DATA
Location 10
Unit 2
Test No.
10/2 -/
10/i-lZ
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Date
Time
ISZ.O
Steam Flow, Ib/hr
•23,3,020
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Final Steam Temp. Before At temp. , °F
Final Steam Temp. After Attemp., °F
•7-87
•755
Burner Gas Press. , psig
Black Liquor Solids, percent
Main Dissolving Tank Density
Percent 0,/Percent Combustibles
4,2.
Total Air Flow, percent
7O
65. 5
72.
Primary Air Flow, percent
Black Liquor Flow to Burners, GPM
ISO
Secondary Air Flow Damper pos. % open
so
50
Gas Flow to Recov. Boiler, SCFK
o
Black Liquor to Burner pressure, psig
ZO
Black Liquor to Burner temp., "F
ZStf
F.W. Temp., "F (typical)
Steam A.H. Air In, °F
110
115
IIS
Steam A.H. Air Out, "F
Boiler Gas Out, "F
-775
-7SO
L.H. Cascade Evap. Gas Out, °F/R.H.
$00
"boo
East Econ. Gas Temp., "F/Mest Econ.
. B
Primary Air Pressure, in. H.O
3.8
F.D. Fan Disch. Pressure, in. H,0
L.H./R.H./New Case. Evap. Motor Load, %
Black Liquor Burner In Service
COBBnent8s
eUrvj-e>rf"
at" ml-ef "fe
542
-------
OPERATING DATA
Location 10
Unit 2
Test No.
I0/2.-H
Date
Time
/2-Z./
Steam Flow, Ib/hr
Steam Press., psig
Final Steam Temp. Before Attemp., °F
860
Final Steam Temp. After Attemp. , *F
Burner Gas Press. , psig
O
Black Liquor Solids, percent
fcZ.
63.5
Main Dissolving Tank Density
M65
Percent 0, /Percent Combustibles
JO.D05
5 10.05
'.kla.QS
Total Air Flow, percent
-. s
•72,5
93
65
Primary Air Flow, percent
Black Liquor Flow to Burners, GPM
zot
'Secondary Air Flow Damper pos. % open
50
Gas Flow to Recov. Boiler, SCFH
O
Black Liquor to Burner pressure, psig
IS
1 5
Black Liquor to Burner temp., *F
2.53
F.W. Temp., °F (typical)
Steam A.H. Air In, °F
IOO
ico
teo
I GO
Steam A.H. Air Out, °F
WO
Boiler Gas Out, "F
L.H. Cascade Evap. Gas Out, "F/R.H.
"&0 3)5
East Econ. Gas Temp. , *F/West Econ.
L.H. Precip. Gas Out/R.H. Pracip., °F
300
too
300
Economizer Water Outlet, °F
400
mo
I.D. Fan Inlet Draft, in. H.O
-2,
L.H./R.H. Precip. Out Draft, in. H.O
Economizer Out Draft, in. H.O
-5,0
-S.3I-S.J
-2. 1
-E.O
Economizer In Draft, in. H.O
-0.5
-0.5
Boiler Inlet Draft, in. H.O
-O.tJ
Furnace Draft, in. H.O
— Oi 2>
-0,3
-0.3
Secondary Air Pressure, in. H.O
6-0
S.7
Primary Air Pressure, in. H.O
r.D. Fan Diaeh. Pressure, in. H.O
z,-?
2>.o
L.H./R.H. /New Case. Evap. Motor Load, %
Black Liquor Burner In Service
6
6
Comment.!
543
-------
OPERATING DATA
Location 10
Unit 2
Test No.
Date
Time
Steam Flow, Ib/hr
Steam Press., psig
Final Steam Temp. Before Attemp., "F
Final Steam Temp. After Attemp. , °F
Burner Gas Press. , psig
Black Liquor Solids, percent
Main Dissolving Tank Density
Percent 0,/Percent Combustibles
Total Air Flow, percent
Primary Air Flow, percent
Black Liquor Flow to Burners, GPM
Secondary Air Flow Damper pos. % open
Gas Flow to Recov. Boiler, SCFH
Black Liquor to Burner pressure, psig
Black Liquor to Burner temp. , °F
F.W. Temp., °F (typical)
Steam A.H. Air In, °F
Steam A.H. Air Out, °F
Boiler Gas Out, °F
L.H. Cascade Evap. Gas Out, "F/R.H.
East Econ. Gas Temp., °F/West Econ.
L.H. Precip. Gas Out/R.H. Precip. , "F
Economizer Water Outlet, *f
I.D. Fan Inlet Draft, in. H.,0
L.H./R.H. Precip. Out Draft, in. H,O
Economizer Out Draft, in. H_O
Economizer In Draft, in. H,O
Boiler Inlet Draft, in. H..O
Furnace Draft, in. H^O
Secondary Air Pressure, in. H.,0
Primary Air Pressure, in. B.O
F.D. Fan Disch. Pressure, in. H,0
L.H./R.H. /New Case. Evap. Motor Load, %
Bla.ck Liquor Burner In Service
J0/2.-JV-
?-2^-7£>
moo
Ib^^ooo
•Zt+O
0
l*)^
SO
O
IS
2-SO ,
—
too
AJotwJodKJVvj
-75&
3/5 3/5
(oOO bt&
ZZO *co
tfIS
-2,6?
-4.5 -4,5
-2,0
-0,55
-O.2.
-o.z.
6.0
3,0
S.o
Sol 50 140
7
1 1
1
-
1 1
1
i
1 1
Comments:
-fcrf jfr £$P
544
-------
OPERATING DATA
Location 10
Unit 2
Test No.
iofe-1
IC/2.-/S
IO/2-/5
Date
Time
Steam Flow, Ib/hr
Steam Press., psig
•950
Final Steam Temp. Before Attemp., CF
375.
Final Steam Temp. After Attemp., CF
Burner Gas Press., psig
O
0
0
Black Liquor Solids, percent
67
67
Main Dissolving Tank Density
I'll
Percent O.,/Percent Combustibles
3, -
10.05
.qslo.Qs
Total Air Flow, percent
"74. 5
-75
13.5
Primary Air Flow, percent
V-Z-
43
Black Liquor Flow to Burners, GPM
Secondary Air Flow Damper pos. % open
Gas Flow to Recov. Boiler, SCFH
o
&
O
O
Black Liquor to Burner pressure, psig
17
Black Liquor to Burner temp., °F
F.W. Temp., "F (typical)
Steam A.H. Air In, °F
ICO
Steam A.H. Air Out, °F
Boiler Gas Out, "F
L.H. Cascade Evap. Gas Out, "F/R.H.
i/O 3/S
East Econ. Gas Temp., °F/West Econ.
L.H. Precip. Gas Out/R.H. Precip., 8F
Economizer Water Outlet, °F
I.D. Fan Inlet Draft, in. H;0
3.O
L.H./R.H. Precip. Out Draft, in. H^O
-s.o
-S. /| -
Economizer Out Draft, in. H;0
-2
Economizer In Draft, in. H..O
-0.75
-O 16
Boiler Inlet Draft, in. HO
-O.S
-0.3
-0,5
Furnace Draft, in. H.,0
-O.Z
-0,3
-<5% 3
Secondary Air Pressure, in. HO
O
&.O
Primary Air Pressure, in. H^O
3.5
3.5
3.
. j
F.D. Fan Disch. Pressure, in. HO
8-5
L.H./R.H./New Case. Evap. Motor Load, %
so
Black Liquor Burner In Service
7
Comments:
545
-------
OPERATING DATA
• Location 10
Unit 2
Test Mo.
Date
Tine
\ 550
Steam Flow, Ib/hr
z; Sv
Steam Press., psig
&SO
^55
Final Steam Temp. Before Attemp. , °F
%&&
Final Steam Temp. After Attemp. , °F
^2,3
Burner Gas Press. , psig
Black Liquor Solids, percent
Main Dissolving Tank Density
1,16;
Percent 0, /Percent Combustible*
10.OS
Total Air Flow, percent
10
69
Primary Air Flow, percent
Black Liquor Flow to Burners, GPM
Secondary Air Flow Damper pos. % open
65
Gas Flow to Recov. Boiler, SCFH
Black Liquor to Burner pressure, psig
Black Liquor to Burner temp. , °F
Z.SS
zss
ZSS
F.W. Temp., °F (typical)
Steam A.H. Air In, °F
\oo
Steam A.H. Air Out, »F
2LS5
260
ZSS
Boiler Gas Out, "F
L.H. Cascade Evap. Gas Out, "F/R.H.
East Econ. Gas Temp., •F/Wett Econ.
6/5
535
5 70
L.H. Pracip. Gas Out/R.H. Precip. , *F
Z10 215
Z70 Z95
Economizer Hater Outlet, °F
I.D. Fan Inlet Draft, in. H.O
-3.0
L.H./R.H. Preeip. Out Draft, in. H.O
-5,2 -5.1
-S.QhStS
-s,o-s,
-------
LOCATION 10
UNIT 2
FUEL (BLACK LIQUOR), ANALYSIS
3t 10/2-2
Organically Combined Elements
Carbon
Hydrogen
Sulfur
Nitrogen
Oxygen (by difference)
Sodium
Inorganic Constituents
Sodium Carbonate (Na0CO,)
t. ; J
Sodium Sulfate (Na^SO^)
Sodium Chloride (NaCl)*
Sodium Hydroxide (NaOH)
Sodium Sulfide (Na2S)
Moisture (
August 31, 1976
21.07 % by weight
2.38
0.19
0.04
16.16
7.13
5.62
10.66
1.25
not present
not present
35.5
^determination not requested, but required for constituent balance
Gross Heat of combustion, BTU/lb
-4117-
The sodium listed under organically combined elements is probably present
as the salt of organic acids. This sodium was calculated by subtracting the
inorganic salt sodium from the total sodium.
547
-------
LOCATION 10
UNIT 2
FUEL AND SMELT ANALYSES
Carbon , %
Hydrogen, %
Sulfur, %
Sodium, . %
Nitrogen, %
Oxygen, % .
Total
Gross heat of combustion,
Btu/lb
Inorganic constituents
Na2C03, %
NaOH, %
Na2S04, %
Na.S, % -
NaSH, %
NaCl, %
Moisture , %
Total .,-.-,... ;
Black
Liquor
23.65
2.36
2.44
11.56
0.06
8.43
48.50
3911
14.9
—
4.26
N.D.
1.01
31.33
51.50
Black Smelt
Liquor 9/15/76
23.80
2.55
1.84
8.56
0.06
15.49
52.30
4133
13.6 67.68
21.44
4.36 1.68
N.D. N;.D.
1.13
1.09 2.55
28.65 5.52
47.70 - 100.00
88.40
N.D.
0.98
N.D.
8.05
2.57
N.D.
100.00
N.D. = not detected
548
-------
Test M
Onit Mo.
PARTICUIATE EMISSION CALCULATIONS
- / Data 2~W?(p Location < O _
Engr .
« Sampling Train and Method
Pitot Factor, Fs
Barometric Pressure,
in. Hg
Tot. Liquid Collected, V JgtS.?? ml 'Total Particulate,
Velocity Head, ApO.075 iwg Stack Temp. , Ts /g/^ *R Stack Area, As?3>.75 ft2
Sample Volume, Vm2.%.2>/ ft.3 Stack Press., Peg— "Z. I iwg Excess Oj, XO % 3-6 %
Orifice Press. Dif f . ,
Sample Time, 6 *7 S min Nozzle Dia.,
•1. Sanple Gas Volume Vm - 0.0334
iwg stack Gas Sp. Gravity, Gs l>6l
Tem
28.
n.d.
in. Meter Temp., T —
+ H/13.6)
2. Hater Vapor Vw - 0.0474 V,
sta ic
3. Moisture Content Bwo " Eq. 2/(Eq. 1 + Eq. 2)
4. Concentration a. C - 0.0154 Mn/Vm . .
sta
b. C • 2.205 x 10"6 Mn/Vm ^
c. C - Eq. 4b x 16.018 x 103
5. Abs. Stack Press. Ps - Pbar x 13.6 + Psg
6. Stack Gas Speed Vs - 174 Fs /APTs Jj&- x ^gSfi
7. Stack Gas Flow a. Qsw » Eq. 6 x As x —— " T^T
Rate « 70°F TB w/
b. Qsd • Eq. 7a x (1. - Eq. 3)
6. Material Flow
10. Emission
11. % Zsokinetic
Ms - Eq. 7b x Eq. 4b x 60
J—l — *w^w/ ^•w* ^ " t***4-~*
a. E • Eq. 4b x Fe x Eq. 9
b. E - Eq. 4c x Fa x Eq. 9 x 1000
14077
I .
6 x Vs x Pa x Dn
2'.
t
Fe SC Feet/104 Btu
Fm SC Meters/104 joules
Oil
92.2
0.002475
Gas
67.4
0.002346
Coal
98.2
0. 002636
-------
Test
Dhit Mo. "2-
PARTICOLATE EMISSION CALCULATIONS
Date ^-T.-1-7C< Location lO
Engr
.'0/2- /
sampling Train and Method
Pitot Factor,
Barometric Pressure, P.>-°'S3
Hg
gm
Tot. Liquid Collected, V 275«^7 ml "Total Particulate,
Velocity Bead, flpQ'O73 iwg Stack Temp., Ts_/O/_3__»R stack Area, As?V75_ft2
Sample Volume,
stack Press., Psq~2' / iwg Excess Q , X0%3»8
Orifice Press. Diff., H
iwg Stack Gas Sp. Gravity,
Sample Tine, 6 "75
•1. Sample Gas Volume
2. Water Vapor .
3. Moisture Content
4. Concentration a.
b.
c.
5. Abs. Stack Press.
6. Stack Gas Speed
7. Stack Gas Flow a.
Hate 0 70*F
b.
8. Material Flow
9. X0_ factor
10. Emission a.
b.
11. % Isokinetic
min Nozzle Dia., Dn^'*'^ in.
Vm . . - 0.0334 Vm{P. '+ B/13.6)
•Co * Pflr
Wstd • °-0474 Vlc
Bwo - Eq. 2/(Bq. 1 4 Eq. 2)
C - 0.0154 Mn/VmD-
^ ' ^7 5 grains/DSCF
O'OQOSS ' lb/DSCP
9* SD grams/DSCM
L4O?><%£? in. w, abs.
l"L"72,Ci> ft/min
5S 'i'iZ WSCF/min
^O S 7S DSCF/min
/^/2 lb/hr
/ b,biw^ M T\
n • •** •
8.10~ Ib/MMBtU
J *^ 8 1 ng/ j oule
(OOfl^l %
6 x Vs x Ps x On
Fe SC Feet/104 Btu
Fm SC Meters/104 joules
Oil
92.2
0.002475
Gas
87.4
0.002346
Coal
98.2
0.002636
Liaoor
o.
•Multiply Vmctd by 530/TB(*R) if meter not temp, compensated.
Data Sheet 6002-4
550
-------
PARTICULATE CALCULATION SHEET.
Test Mo..
Box No.
Date
Test Craw
Location
Test Description
Sample Probe Position
Dry Gas Mater
Final
Initial
Total
(ft3)
5?
££.
Final
Initial
A vol
Znpinger Water Vol (ml)
340
100
2^0
64
=35
8. Gel
68* .MO
fe~?e>W3
Total
I*?"
Beaker Mo.
8
Filter
No.
•7
Blank
No.
ft
Tare
Wt.
1 IO&OH-J
?? '65
2 ioo.
-------
PLANT —
METHOD 5 CONTROL CONSOLE READINGS
LOCATION / Q
OPERATOR —
DATE
RUN NO. \e>/T.-l
SAMPLE BOX NO. /
METER BOX NO. 7"
1ETER H —
: FACTOR"! ——
-• T'J"
£•
1 f
\
AMBIENT TEMPERATURE
BAROMETRIC PRESSURE
ASSUMED MOISTURE, %
HEATER BOX SETTING
PROBE LENGTH, IN.
NOZZLE DIAMETER, IN. _, ,
PROBE HEATER SETTING =
SCHEMATIC OF STACK CROSS SECTION
Traverse
Point
Number
'TOTAL
\Vrnr\rr
ClocK.
u'JZ?'
1053
1108
//Z3
H58
1/53
>ZoS
Static
Pressure
(P8)r
-2./
-2./
-Z. /
-?./
-2./
-2./
Stack
Tempera-
ture
S^>
5^0
^/5
553
Velocity
Head
&*.tf?
'S09.92
IStS.Zf
/S20,
Op
—
—
no
US
izo
'2.S
i
AVG.
„,*.'
Sample
Box
Temprta-
ture
°F
5'S
3co
3^0
320
320
320
.-
RVR .
Temperature
of Gas
Leaving
Condenser on
jast Impinger
•F
go
ffs
70
68
69
75
!
i
•
[ -
i
'•
01
en
-------
PLANT
LOCATION
OPERATOR"
DATE e»-
METHOD 5 CONTROL CONSOLE READINGS
RUN NO. IQ/Z-JS
SAMPLE BOX NO. ~
METER BOX NO. 5T~~
1ETER H '—
: FACTOR"! "
* 3P-\ **-
f
? '
«-8'-t^55
8'
i
\
\
*
AMBIENT TEMPERATURE
BAROMETRIC PRESSURE '
ASSUMED MOISTURE, % '
HEATER BOX SETTING '
PROBE LENGTH, IN.
NOZZLE DIAMETER, IN.'
PROBE HEATER SETTING"
SCHEMATIC OF STACK CROSS SECTION
Traverse
Point
Number
TOTAL
writer
Sfflnplij^
^^
f^TMhi.
C locK
Tin***
Hrt.
WL<=>
1^45
'^45
'*SS
ISos
'S/5
iszs
/S^S
/sss
/6os
Static
Pressure
(P8),
In. 'Hg.
ih^obu
Stack .
Tempera-
ture
(T8) »F
3^0
3tfO
3co
3so
Be»o
3oo
3oo
rt ^y
Zf8
^?8
—
-
z&%
3o
Velocity-
Head
.5
K5
I-S
A3
'•S
2d >nm>
AS
'•5
—
Pressure
Differen-
tial Acros
Orifice
Meter
(AH) ,
In. H.O
o.*?s
o.as
O.'JO
0.90
o.?o
O. ft3
SS?/.96
S6CO.OQ
S60&00
5^/6.5o
S6Z3.30
S6S/.SO
%3?flO
ttx" v*/tt/*>
Si 39, so
56w7.«ao
56 S#
Gas Sample
Temperature at
3ry Gas Meter
Inlet
(Tmin.)
°p
e by ^
Outlet
(Tmout'
•P -
—
— •
^0
92.
^^
/
-------
ANDERSEN CASCADE IMPACTOR DATA
Test No.
Impactor No.
I
Stack Temperature
Location
Owner
Nozzle Size
°F Inipactor Flow Rate
Filter No. —
CFM
Plate
Tare (g)
Final (g)
Net (g)
Cum. %
BCD
70,0
-^.0757
0,0065
01
tn
O .
8
0^001®
3.S95
Back Up
Filter
0,0015
Data Sheet 6002-5
-------
Project!
Pat*. %
VELOCITY TRAVERSE
Test Description!
1 O
Stack Cross Section
Uniti_
Test<_
Fueli Sa/fl-C £
I0/2.-Z.
Personnels
Barometric Press, (in. Bg)t
Absolute Static Press, in Stack (in. Bg):_
Pltot Tube Coefficient!
(P.)
Time
Traverse Point
Port Depth
'4.**!
\ "
i ^"
z "
z.fc"
3 "
r'
Velocity
Bead
(in. B,0)
AP
C?.|
0.0
-------
Project!
VELOCITY TRAVERSE
Test Description!
Location! / O
Ifctti "2.
Tests
StacX. Cross Section
Personnelt
Barometric Press, (in. Bg)s
Absolute Static Press, in Stack (in. Hg):_
Pitot Tube Coefficients
(P.)
- 85.48
1/2
Tlae
Traverse Point.
Port Depdrf
-
*+,
0.5
1.0
1.5
2.0
1.Z
^.0
Velocity
Bead
(in. H,0)
AP
o,|
O,(06
O.07
0,06
(5.07
0.
Gas Teap.
CR)
Ts
Molecular
Ht.
"s
Velocity
(ft/seci
vs
/9,2
Cone.
(% Dry)
6002-11
556
-------
Project!
oat*.
VELOCITY TRAVERSE
Test Descriptions
location! / 0 Stack Cro«» Section
Bniti
-i :::::::
Testi 1 0 /z — i*f personnel! ::.::::
Fusli fcktK £'"«,«« V
Barometric Frees, (in. B
Absolute Static Press, i
Pitot Tube Coefficients
V8 - 85.4. C,
MM
0920
—
—
—
—
&Wt>
.
tt). T,^. $7
n Stack (in. Bali '2-<3'~7G (P.)
o,S3
(CU)
r^r
LVsJ
Traverse Point
Port Depth
1
z
7.
1.
T.
T.
*
/'
2'/"
3'Z"
Vs"
S'«f-
6'S"
Velocity
Bead
(in. B,0>
AP
'.^>
/. i
1.3
1,2.
I'l
'•I
Gas Teap.
(»F)
3O
SCO
3oo
110
?S\0
240
Gas Tenj>.
(•W
«s
•750
if
™- o •
Molecular
Wt.
"s
^-7.^^
Velocity
(ft/sert
Vs
IS
•
02
Cone.
(» Dry)
"7,0
6002-13
55-7
-------
Date
K V B. INC.
Test
- 3
TEST NO./P/Z-S UNIT NO.Z
SOx DATA SHEET
B/AC&
*^ LOAD I
klb/hr tgLoeation
Box Mo.
Time
Temp, in Gas Meter
Press, in Gas Meter
Meter Reading
Barom. Press.
Percent Oxygen
N2 Purge Time
\0e\
z.:n$
^7.
0
o/
^:^«f
Caiculation:
Excess 02 S i I
or
ppm
- (A " B) x
T) x
A * Ml of lead perchlorate used for sample
B « Ml of lead perchlorate used for bland
N » Normality of lead perchlorate titrant
F * Dilution factor
T » Average temp, in gas meter
V - Volume of gas sample ft3
P » Barometric pressure
p - Pressure in gas meter
Concentration,C/ ppm
,gjn/d8cm
B - aT 2090 1
B0.9-XOL, I
where L J
Emission-,E, g/Meal
Ib/MBtu
ng/J
C - pollutant concentration, g/dscm
F, volume factor - dscm/10 cal
jascf/104
from red. Beg. 9/11/74 p 32856
so
4.60
HO
I4?,
O
so
0.0/S7?
60-14
rev. 1/2/75
553
-------
Date -
K V B. INC.
T..t
- 5
TEST NOJO/L-SUNIT HO. T.
SOX DATA SHEET
!>Itt
vq
-
lol
Z ', Si.
o%
-
Z,<9£&
- •
-
—
"ioC,
*\n
S&
-
0,000
**.?«-
^••7
-
aoc.
4'.0S
^4>
—
Z.ooo
«.
_
i
(A - B) x N x F x (460 + T) x 24
* * 2
A - Ml of lead perchlorate used for sample • Wj $
B • Ml of lead perchlorate used for bland • "
N • Normality of lead perchlorate titrant •0>O)^7?
P • Dilution factor » / O
T • Average temp, in gas meter • $~(o
V • Volume of gas sample ft3 • ~~"
P » Barometric pressure • ^-^'8?
p • Pressure in gas meter • O
Concentration, C, ppm • *4 , 1
iam/d-om .
Eml«»ion-.Ef g/Meal •
B • Cn 2090 1 - -Ib/MBtu *
B0.9-xCkl
wbar* L ^J ng/J - .
C • pollutant concentration, g/dBcm .
T. • volume factor • dscm/10 c«l
d«cf/lo4 Btu
from Fed. Reg. 9/11/74 p 32856
803
/O,i/
4, (,
0,01 S7 8
Ov
?tp
2,<50O
—
' —
1199
t
60-14
Z«v.
80X
1/2/75
559
-------
Date
K V B. INC.
Test Mo. ID/2-
SOx DATA SHEET
TEST
«%
-g UNIT NO. 7. FUELii
LOAD —
b/hr /QLocation
Box NO.
Time
Temp, in Gas Meter
Press, in Gas Meter
Meter Reading .
Barom. Press.
Percent Oxygen
N2 Purge Time
Ob
/£/O
so
*
V » Volume of tras sample ft3 - 2,*>6»2
P « Barometric pressure • "in iZv
p - Pressure in gas meter « ^
Concentration ,C, ppm » ''•C-5 __
ian/dscm .
• Emission -,E, g/Mcal •
E - of 2090 I Ib/MBtu "
ko.B-xoJ
r ^^2 1 *
C • pollutant concentration, g/dscn .
Fr volume factor * dscn/10 cal
dscf/104 5^
from Fed. Reg. 9/11/74 p 32856
so3
3 •?»
—
—
/ O
q^, 5
—
—
—
m,s?
60-14
rev.
sox
1/2/75
560
-------
TABLE TRACE SPECIES AND ORGANICS SAMPLING CONDITIONS
LOCATION 10 - BLACK LIQUOR RECOVERY BOILER
TS & O Run No.
Test Nuinber
Date
Port Location
Velocity, m/s (f/s)
Stack Temp., K (°F)
Oxygen Content, % dry
Moisture, %
Sample Time, min.
Cyclone Flow, awcmm (awcfm)
Isokinetic Rate, %
Oven Temperature, K (°F)
XAD2 Temperature, K (°F)
Meter Temperature, K (°F)
Nozzle Size, mm (in.)
No. Filters Used
Sample Flow, dry, scmm (scfm)
Volume Collected, dry, scm(scf)
Particulate Catch, g
Solid Particulate, ng/J
(lb/106 Btu)
1
10/2-10
9/15/76
Furn. outlet
5.49 (18.00)
555 (539)
4.7
25.11
38.6
0.081 (2.852)
113.6
478 (400)
306 (91)
308 (95)
19 (0.75)
2
0.0424(1.497)
1.636(57.74)
17.7646
4294 (9.99)
2
10/2-12
9/16/76
Furn. outlet
7.70 (25.24)
546 (523)
7.8
20.99
25.8
0.115 (4.064)
91.9
478 (400)
307 (93)
313 (104)
19 (0.75)
2
0.0516(1.819)
1.330(46.92)
8.4520
3180 (7.2)
3
10/2-14
9/22-23/76
ESP outlet
24.10 (79.06)
411 (279)
7.5
34.79
300
0.120 (4.224)
97.4
- 478 (400)
321 (119)
307 (92)
9.53 (0.375)
1
0.0466(1.644)
13.977(493.2)
0.4928
16.8 (0.039)
4
10/2-16
9/27/76
ESP outlet
22.87 (75.00)
407 (273)
7.45
31.15
301
0.115 (4.049)
97.7
478 (400)
296 (73)
305 (89)
9.53 (0.325)
1
0.0472(1.666)
14.213(501.5)
0.4334
14.5 (0.034)
tn
o
-------
TABLE
BLACK LIQUOR RECOVERY BOILER PROCESS FLOW RATES FOR SASS TESTS
fO
Test
Sample Position
Liquor Vol. Flow,
m3/s
(GPM)
Liquor Spec. Gravity
Liquor Mass Flow, g/s
Sodium in Liquor, %
Sodium Input, g/s
95% Smelt Na Output,
g/s
Sodium in Smelt, %
Smelt Mass Flow, g/s
Liquor Heat Input, MW
(106 Btu/hr)
Excess O_, %
Stack Flow, Nm3/s, dry*
(dscfm)
10/2-10
Furn. .outlet
0.0129
204
1.18
15,185
19.8
3,007
2,856
43.7
6,536
138
(471)
4.7
54.6
115,700
10/2-12
Furn. outlet
0.00852
135
1.17
9,964
19.8
1,973
1,874
43.7
4,289
90.5
(309)
7.8
44.3
93,831
10/2-14
ESP outlet
0.0124
197
1.169
14,528
16.3
2,368
2,250
42.9
5,244
140
(477)
7.5
66.8
141,600
10/2-16
ESP outlet
0.0114
180
1.168
13,263
16.3
2,162
2,054
42.9
4,787
127
(435)
7.45
60.7
128,700
*stack flow based on 3.065xlO~7 dNm3/J (11420 DSCF/10 Btu) at zero excess
oxygen
-------
Project i
Date: q
KVB/ INC, TRACE SPECIES AND ORGANICS SAMPLING DATA
Personnel: f4?£lno*j .TWySon j Barometric Press i
Location:
Test: I
O/1. —
I Q
Fuel: 8/AcK
e. 8nic< Probe Nozzle Diameter (inches):
_ Absolute Static Press, in Stack
Pi tot Tube Coefficienti O.9S
— f
(Dn)
(PS)
(Cp)
TIME
Real
Elapsed
Traverse
Point
Depth
Pitot
AP
(in H20)
Orifice
AP
(in H20)
Cum.
Meter
Volume
(ft3)
Punp
Suction
(in. Hg)
TEMPERATURE (»P)
Stack
Probe
XAD-2
Inplnger
Out
Oven
Meter
In/Out
°2
Cone.
% dry
40Z.W2O
63
1 0
O.OS
n.s
O.C»S
Si-z-
"'I
93
CJ1
o>
d cd-
|O
1
r.iw
1-1-1
o i_
0 +0
4M.
O.OS
1 O
o.os
8
aos
IOO
2Z.S
t
mm
£
KVB 6002-12
-------
KVB, INC, TRACE SPECIES AND ORGANics SAMPLING DATA
Projectt
Date:
Location!
Personnel!
G) -\(y-~J& f
MCCVK-O^ %
Barometric Press : x
*~J
Onit«»'£» £'£• «tcO*ry £b!>6u<" Probe Nozzle Diameter (inches) i "— ' *
(Dn)
Test: l_>/2. — '"2. w Absolute Static Press, in Stack (in. Hg) i ~~~" (Ps)
Fuel: Pi tot Tube Coefficient:
cn
O5
TIME
Real
'35*?
W&Cp
/f/3
l*lb
1507
»5/o
»5/Z
/5/y.
• 5/6
Elapsed
O
1
,4
/£.5
£>
—
5
—
9,3
Traverse
Point
Depth
l&Kfc
•i
"
"
Pitot
AP
(in H2O)
0,0.S^
—
5//.3co
—
smij
(Cp)
Pun^>
Suction
(in. Hg)
&. )
IZ.O
Zo.o
z^.o
c/K-»«*Ki'f
5..0
—
10.0
• —
•z.s,o
TEMPERATURE ( • F )
Stack
513
^
sn
—
*_
—
—
So 8
—
—
Probe
MOO
4M
401
—
3«?5>
— .
3*76
—
—
XAD-2
%
\eo
9S*
—
S7
—
-------
Project!
Date.
Location: I C
Onitt6J«t£/.lfr
Test./g/2. -/*/
Fuel i
KVB, INC. TRACE SPECIES AND ORGANics SAMPLING DATA
Personnel t VUao Barometric Press i
^
&>»_»< Probe Nozzle Diameter (inches) t
Absolute Static Press, in Stack (in. Hg) t
Pitot Tube Coefficient i
_(Dn)
_(Ps)
.(Cp)
TIME
Real
Elapsed
Traverse
Point
Depth
Pitot
AP
(in B20)
Orifice
AP
(in H2O)
Cum.
Meter
Volume
(ft3)
Pump
Suction
(in. Hg)
TEMPERATURE (*P)
Stack
Probe
XAD-2
Inpinger
Out
Oven
Heter
In/Out
Cone.
% dry
'•3
I.-75
S2Z.IOOZ
78
170)
IS
116
1-7/6
30
10?
en
o«
en
&O.-7CCO
S.5
107
92
60
S.5
toB
too
75
1,3
S.S
100
1/3
KX.
90
'•3
6-77.?
6.0
/zo
•70S.Z
6,2
100
IOZ
6.T
105
J.S
705,2
6,7.
If
1.3
6,5
7?
WO
wo
1*5
n
75 g. 5
597
/SO
n
6,9
ILQ
82.
396
1135
165
7.0
1*7
7?
I15&
M
'.3
837. /
-7.0
127
77
11
II
1.3
1.9
to
KVB 6002-12
-------
Project!
Date» 3-
KVB, INC. TRACE SPECIES AND ORGANics SAMPLING DATA
PersonneltP/otrSSa^ CWr Barometric Pressi
Locations /
Onitt 6/«cK /..
Test: tO/Z-/V
Fuel i 6/ack?
Probe Nozzle Diameter (inches)t
Absolute Static Press, in Stack (in. Hg)i
Pitot Tube Coefficients
_
-------
Project!
Datei
KVB, INC. TRACE SPECIES AND ORGANics SAMPLING DATA
Personnel i Barometric Press i
Locations
Onitt!
; Iced
Bat Us Probe Nozzle Diazeter (inches)
Test: lO/'2~—
Fueli
.(On)
Absolute Static Press, in Stack (in. Hg)t
Pitot Tube Coefficient!
_«*)
TIME
Real
Elapsed
Traverse
Point
Depth
Pitot
AP
(in B2O)
Orifice
AP
(in H20)
CUB.
Meter
Volume
(ft3)
PUMP
Suction
(in. Hg)
TEMPERATURE (*P)
Stack
Probe
XAD-2
ZMpinger
Out
Oven
Meter
in/out
Cone.
% dry
'•!£>
/,6S
•3
2S
'3
t.zo
091.^00
S.5
•77
US?
'.65
in.
6.O
17
§s
CD
•vj
1212.
1,-L
'.4s
7Z
IZ/Z7
•2--7S
75
"7
-75
II
/./s
/.6S
s.s
400
87
•73
S7
S.-7S
uoz.
87
/zo
.
5.75
398
70
73
398
M
1
-------
Project:
Date: ~-
KVB, INC, TRACE SPECIES AND ORGANics SAMPLING DATA
Personnel» ri a r>*S S^ t Barometric Press i "
Locations
S9'^*"probe Nozzle Diameter (inches) i
w (On)
Testi \o)"2.-lC* Co>o-/<»t«-gd. Absolute Static Press, in Stack (in. Hg) i ——' (Ps)
Fuel i &/a.C^ l~ ' fiUo f Pitot Tube Coefficients ' (Cp)
TIME
Real
Elapsed
Traverse
Point
Depth
Pitot
AP
(in H2O)
Orifice
AP
(in H20)
Cum.
Meter
Volume
(ft3)
Pump
Suction
(in. Hg)
TEMPERATURE (*F)
Stack
Probe
XAD-2
Inpinger
Out
Oven
Meter
In/Out
Cone.
% dry
M
MS
"V70.0D
1-4 O2.
-77.
•75
10
cn
O5
oo
MS
Z--7Z
M
2--7Z
15
^oo
II
8-O
woz
•7-7
153,5
1*41
• 1
8,1
•70
»5SO
M
S66.9
2.-7Z
-76
/.2.O
M
-7Z
17
93
u
S.z
^03
-7Z
II
s.z
ZT73
400
-------
TRACE SPECIES AND ORGANICS TEST
SAMPLE RECOVERY LOG
Test No.
Date 9 - JS-^fe Location lO
Sample Port Position
'° *ReC\PtTATTC)g-
^^
Container
Number
8.40
_iii.
tit
Sample Description
?i Jl Sov-tfiS
Xu.
I >
L »~ILT V^oiifc. UJkft
L,T>
"Bute L\<»o<«.
L - 1. "Tfc*.)viV.\
.\oo\js
— Q. T
Container
Type
oz.
Net
wt/vol.
3.6. ant,
3>.92*3 a.
jjy»\
5^5 Ji
_5&is
Comment
ViT.
5
4 \2-
Data Sheet KVB 6002-15
569
-------
Test No.
TRACE SPECIES AND ORGANICS TEST
SAMPLE RECOVERY LOG
Date 9- 15-% Location (Q
Sanple Port Position
Container
Number
Sample Description
Container
Type
Net
wt/vol.
Comment
!££>
J J
. 1
S&7
APft
2. Pit-Tea.
lee. ^
£$2.
S
UZ
£.&
£05
10-7
*3
F Le "to "BtitiJees
6 -
Q&
L •" \ Ttkikl Li
\ Lio
A.UA.L..
Data Sheet KVB 6002-15
570
-------
TEST 10/2-10
Sample ;No.
389
380
391
287 • 288
F
243
292
205
G
H
304
201 a
297 ^
227
1000
KVB
POM'S
-------
INLET OF PRECIPITATOR TABLE Tcst fj.o/2-10
POLLUTANT SAMPLE NUMBER
Antimony
Arsenic .
Barium
Beryllium
Cadmium
Calcium
Chromium
Cobalt
Copper
Iron
Lead
Manganese
Mercury
Nickel
Selenium
Tellurium
Tin
Titanium
Vanadium
Zinc
Chloride
Fluoride
Nitrates
Sulfates
389+
<2.o
XI -
TO
0-2-
•H
•2.0Q
2.1
*
3.U
2.10
110
TS
It
S •
^0
<0./
10
2fl
8
8
2-0
no
18
31
'••a
^,00
CSO
.3.
205*
-------
INLET OF mciPITATOft
TABLE
Test #10/2-10
POLLUTANT
SAMPLE NUMBER
Antimony
Arsenic
Barium
Beryllium
Cadmium
Calcium
Chromium.
Cobalt
Copper .
Iron
Lead
Manganese
Mercury
Nickel
Selenium
Tellurium
Tin
Titanium
Vanadium
Zinc
Chloride
Fluoride
Nitrates
Sulfates
G*
.o&o
S
<3
o.co
3oSoo
304*
-------
COMMERCIAL TESTING & ENGINEERING CO.
OENEKAl OFFICE*: 191 NORTH LA (AU.E STREET, CHIOAQO, ILLINOIS 10101 • AREA CODE 111 ««-i4»4
Reply lO INSTIUMfNTAl ANAlYStI DIVISION, 14315 WtSt 44TM AVINUi, OOIDCN. COUMADO M4DI, fHONti XO-J7WSI
To, Mr. John G. M1cha1ov1c
Calspan Corporation
Post Office Box 235
Buffalo, NY 14221
P.O. No., 27810
Date: Febnfary 8. 1977
Anal/it: S. Sweeney
Simple No.: Sample A
ELEMENT CONC
Uranium
Thorium
Bismuth
Lead
Thallium
Mercury NR
Gold
Platinum
Iridium
Osmium . •
Rhenium
Tungsten '
Tantalum
Hafnium
Lutetiat
YtterMua
Thulium
Erbium
Hoi ml urn
Dysprosium
NR - Not Reported
All elements not reported
(1-6-77) 389, 380,. 391,
CONCENTRATION
ELEMENT CONC.
Terbium
Gadolinium
Europium
Samarium
Neodymium
Praseodymium
Cerium
Lanthanum .
. Barium ' 8
Cesium
Iodine 9
Tellurium .
Antimony
Tin
Indium STD
Cadmium
Silver :
Palladium
Rhodium
<0.8 ppm weight
287, 288
IN PPM WEIGHT
ELEMENT
Ruthenium
Molybdenum
Niobium
Zirconium •
Yttrium
Strontium
Rubidium
Bromine
Selenium
Arsenic
Germanium
Gallium
Zinc
Copper
Nickel
Cobalt
Iron
Manganese
Chromium
Appiov^oi ^^/
IAD No.,
CONC.
1
*4
63
31
<1
2
<0.7
6
5
36
0.6
49 -
20
7
V/f £*
97-A48-134-05
ELEMENT
Vanadium
Titanium
Scandium
Calcium
Potassium
Chlorine
Sulfur
Phosphorus
Silicon
Aluminum
Magnesium
Sodium
Fluorine
Oxygen
Nitrogen
Carbon
Boron
Beryllium
Lithium
Hydrogen
y^fc^SU-X-^
CONC.
0.7
<24
<1
510
MC
MC
MC
120
210
10
330
MC
-130
NR
NR
NR
9
85
NR
^
^Heterogeneous
574
-------
Reply to
COMMERCIAL TESTING & ENGINEERING CO.
etNCtAl OFriCMl til NOUTM I* lAllt ITMIT, OHIOABO, IUINOI* 10101 • A*(A COM lit Tt*-*4»4
IN1TIUMINTAI ANAlVllt DIVISION. I«JM WIST «IM AVINUI. OOIMN. COlOtAOO M40I. MONIi MMIMfll
To' Hr. John G. Hlchalovlc
Calspan Corporation
Post Office Box 235
Buffalo. NY 14221
.P.O. No., 27810
e»t»l. MA .
SempleNo., SwnpU R ^.g.yy) 292
CONCENTRATION IN PPM WEIGHT
ELEMENT CONC.
Uranium
Thorium
Bismuth
Lead . <9
Thallium
Mercury NR
Gold
Platinum
Ir1d1um
Osmium
Rhenium
Tungsten
Tantalum
Hafnium
Lutetlum
Ytterbium
Thulium
Erbium
Hoi ml urn
Dysprosium
ELEMENT CONC.
Terbium
Gadolinium
Europium
Samarium
Neodymlum
Praseodymium
Cerium
Lanthanum
Barium 9
Cesium <1
Iodine
Tellurium
Antimony
Tin
Indium STD
Cadmium
Silver
•Palladium
Rhodium
ELEMENT
Ruthenium
Molybdenum
Niobium
Zirconium
Yttrium '
Strontium
Rubidium
• Bromine
Selenium
Arsenic
Germanium
Gallium
Zinc
Copper
Nickel
Cobalt
Iron
Manganese
Chromium
^ February 11, 1977
Analyst! S. Sweeney
IAD No., 97-A48-134-05
CONC. ELEMENT
Vanadium
Titanium
Scandium
Calcium
Potassium
3- Chlorine
0.8 Sulfur
Phosphorus
Silicon
Aluminum
Magnesium
<2 Sodium
9 Fluorine
6 Oxygen
8 Nitrogen
<2 Carbon
40 Boron
0.7 Beryllium
5 Lithium
Hydrogen
CONC.
1
. 25
<0.3
MC
37
4
26
37
160
11
190
270
•1?
NR
NR
NR
xprl
0.7
NR
NR - Not Reported
All elements not reported < 2 ppm weight
Approved-.
575
-------
COMMERCIAL TESTING & ENGINEERING CO.
Reply to
ICE*: lit NOHIM L» lAlll ITCEIT. CHICAGO, IIUNOI1 (0*01 • A«EA COOf »ll »<-*4>4
INSTIUMINTAI ANAITSIS DIVISION. 14395 wist «TM AVINUI. GOIDIN, coiot*oo KUOI. maul:
A
To: Mr. John 6. Mlchalovic #
Calspan Corporation ***£
Post Office Box 235
Buffalo. NY 14221
P.O. No.: 27810
fv
lUL^Bk
•M *•••
Sample No.= Sample C (1-6-77) 243, 205. 818, 819, 302,
303, 304 • CONCENTRATION IN Vg/Hll
ELEMENT CONC.
Uranium
Thorium
Bismuth
Lead 0.07
Thallium
Mercury NR
Gold
Platinum
Irldlum
Osmium
Rhenium
Tungsten
Tantalum
Hafnium
Lutetlum
Ytterbium
Thulium
Erbium
. Holmlum
Dysprosium
NR - Not Reported
All element* not reported
Sample was thermally
ELEMENT CONC.
Terbium
Gadolinium
Europium
Samarium
Neodymium
Praseodymium
Cerium
Lanthanum
Barium 0.2.
Cesium
Iodine
Tellurium
Antimony 0.1
Tin 0.03
Indium STD
Cadmium
Silver MC
Palladium
Rhodium
<0.003 yg/raj
ashed 8350 VC for one
ELEMENT
Ruthenium
Molybdenum
Niobium
Zirconium
Yttrium
Strontium
Rubidium
Bromine
Selenium
Arsenic
Germanium
Gallium
Zinc
Copper
Nickel
Cobalt
Iron
Manganese
Chromium
*•
Approved: y
half hour In a
D«te: February 8, 1977
Analyst: S. Sweeney
IAD No.:
CONC.
0.02
0.006
£0.03
9
±3
NR
NR
NR
0.07
0.01
NR
.S
a quartz
crucible prior to analysis
676
-------
COMMERCIAL TESTING & ENGINEERING CO.
ecxtBAi ornctt: «*• MOUTH IA «AIIE ITHEET. CMICAOO. ILIINOI* *o«oi • AMA CODE til 7i«.|4«4
Reply tO INSTIUMENTM AMAirSIS OIVIIION. 1*1)5 WIST 44TH AVENUI. GOLDEN. COIOIAOO M40I. PHONE, lOMTMfll
TO: Mr. John G. Hichalovlc
Calspan Corporation
Post Office Box 235
Buffalo. NY 14221
(V
P.O. No.: 27810
Sample No.: Sample 0 (1-6-77) 297
CONCENTRATION IN PPM WEIGHT
Date: February 8. 1977
Analyst: S. Sweeney
IAD No.: 97-A48-134-05
ELEMENT CONC.
Uranium
. Thorium
Bismuth
Lead
-------
COMMERCIAL TESTING & ENGINEERING CO.
•tNCRAl OrnCU: ttt NORTH LA SAIL! (TRIET, CHIOAOO, ILUNOI* tOIOI • ARIA COOI tit Tt»-MI4
Rep)/ tO INtnUMIOTAl ANAITSH OIVIIION. HM3 WIST 44TM AVINUli OOLMN. COIMAOO *MOI. fUOHt: MM7MS1I
T°' Mr. John G. M1chalov1c Ail^
Calspan Corporation . ^^SfJS^:
Post Office Box 235
Buffalo, NY 14221
P.O. No.: 27810
Sompl.No.: Sample E (1-6-77) 1000
«>•»•' February 8, 1977
Analyst: S. Sweeney
IAD No.: 97-A48- 134-05 ,
. CONCENTRATION IN PPM WEIGHT '..
ELEMENT CONC.
Uranium
Thorium .
Bismuth
Lead
Thallium
Mercury NR
Gold
Platinum
Irldlum
Osmium
Rhenium
Tungsten
Tantalum **19
Hafnium
Lutetian
Ytterbium
Thulium
Erbium
Holmium
Dysprosium
ELEMENT CONC.
Terbium
Gadolinium
Europium
Samarium
Neodymlum
Praseodymium
Cerium
Lanthanum
. Barium 22
Cesium
Iodine
Tellurium
Antimony
Tin
Indium STD
Cadmium
Silver
Palladium
Rhodium
.
ELEMENT
Ruthenium
Molybdenum
Niobium
Zirconium
Yttrium
Strontium
Rubidium
Bromine
Selenium
Arsenic .
Germanium
Gallium
Zinc
Copper
Nickel
Cobalt
Iron
Manganese
Chromium
CONC.
2
6
<13
2
<0.7
24
*54
..',6 ,
<0.7
36
37
*10
ELEMENT
Vanadium
Titanium
Scandium
Calcium
Potassium
Chlorine
Sulfur
Phosphorus
Silicon
Aluminum
Magnesium
Sodium
Fluorine
Oxygen
Nitrogen
Carbon.
Boron
Beryllium
Lithium
Hydrogen
, CONC.
0.7
<24
<1
690
MC
MC
MC
160
250
18
330 ,
MC
MC
NR
NR
NR
34
250
NR
_^
NR - Not Reported
All tltmentt not reported <0.8ppm weight
•Heterogeneous **Probable Contamination
Approv*di
578
-------
TRACE SPECIES AND ORGANICS TEST
SAMPLE RECOVERY LOG
Test No. lQ/g-12 Date 9/lfe/7fe> Location \O -
Sample Port Position \Uu&T
Ou /Uy
Container
Number
Sample Description
Container
Type
Net
Comment
54.1
\lfij
£4
il^T HtXA LAiAll
we
73.U.
tSS
7 224n(
S
\J)Vl
924*1
24UC
22A
LB Dun:
Dot **>
LB
LB 'PA,
ja.
IODZ.
1003
Fffc
Ioo4
946 S- 460
yv^Z
S - S Texiu
L -
- I Foei_
- 4- LIQ.
-^-1- Tfeecese
Data Sheet KVB 6002-15
579
-------
TEST 10/2-12 KVB ANALYSIS DATA
Sample No.
383
328
397
285-286
I
235
291 !'
206
314
315
316
228
229
\ 230
231 .
1002
1003
POM*s PCB's
_
-• • -
'- ' -
0.29 ug/g \W <100 ug/g
<0.2 ug/g^ <0.5 ug/g
• : - i "
50 ug/g 1\S>0 <25 ug/g
<1 ug/g/0 <5 ug/g
<0.2 ug/g/0 <0.5 ug/g
1.26 ug/1 \\^y«\ <1 ug/1
<0.4 ug/1 <1 ug/1
-
-
•. -
<10 ug/g <50 ug/g
117 ug/gy <50 ug/g
Remarks
NES
NES
NES
NES
,
NES
.NES
NES
NES
NES - Not enough sample
I - 241, 242, 244, 245, 247, 248
580
-------
INLET OF PRECIPITATOR TABLE Test Ho/2-12
POLLUTANT SAMPLE NUMBER
Antimony
Arsenic
%arium
Beryllium
Cadmium
Calcium
Chromium
Cobalt
Copper
Iron
Lead
Manganese
Mercury
Nickel
Selenium
Tellurium
Tin
Titanium
Vanadium
Zinc
•t
Chloride
Fluoride
Nitrates
Sulfates
383+
-------
INLET OF PRECIPITATOR
TABLE
Tect f 10/2-12
POLLUTANT
SAMPLE NUMBER
Antimony
Arsenic.
Barium
Beryllium
Calcium
Chromium
Cobalt
Copper
Iron
Lead
Manganese
Mercury
Nickel
Selenium
Tellurium
Tin
Titanium
Vanadium
Zinc
Chloride
Fluoride
Nitrates
Sulfates
314*
o.-z.
O./lo
CO-OZ.
.£
^0.003
o.V
o.os
0.03
.\
/so
8
//o
-------
INLET OF PRECIPITATOR TABLE Test 110/2-12
POLLUTANT ' SAMPLE NUMBER
Antimony
Arsenic
Barium
Beryllium
Cadmium
Calcium
Chromium '
Cobalt
Copper
Iron
Lead
Manganese
Mercury
Nickel
Selenium
Tellurium
Tin
Titanium
Vanadium
Zinc
Chloride
Fluoride
Nitrates
Sulfates
1003+
0.0,, $
.«
•9 ll ? 9
*»•" |fc««"W
1.0,1.0
39,30
8,4»
•5Z.3Z.
1
1
583
-------
Test No. IO/g-14 Date 'S
f
Sample Port Position C\yri_g-r
TRACE SPECIES AND ORGANICS TEST
SAMPLE RECOVERY LOG
Location \Q -
o»4
Container
Number
Sample Description
Container
Type
Net
wt/vol.
Comment
10-L.QxiBS
I'll
JtT
_£32,
3 XJL
IM-J
r-»lrr.
22 T
CxJ
(4)
JH
,
AH
318
281 3
558,4
104*
32A-
fa
loas
loot
U.T Cite. 6/2S
100
Data Sheet KVB 6002-15
584
-------
\1
TRACE SPECIES AND ORGANICS TEST
SAMPLE RECOVERY LOG
(2s
QL
test No. IO/
Sample Port 1
Container
Number
\CCto
1010
lo 1 \
\n\-2.
COOUT
4
L . . A/ /
2.-" Date »/a£-2a/~ft> l«cat
/
^osition CjOTl_£T >-
Sample Description
F Liol5.bop fS^r.)
i^\fV LiaooO. (^/i^
^3 *^ *T f*t^^-l^ ^
1^ ^ '^S L^ IQ ^\^C.
P - 2 PLl£La.
"D "5 Al
1
Cfiil&iKLr S^apiE* &
"l^Citslcr /LlALV2E_
•
:ion Jto — ^
^p'Rccvpn
Container
Type
C*u*SS
H
U
II
\4 /
?*ol
j.
£.Av|
-------
TEST 10/2-14
Sample No.
398
396
279
J
225
293
K
L
N
N
1007
1008
1009
1010
KVB ANALYSIS
POM'S
-
•
-
0.37 ug/1. VJ%
613 ug/i \wtf
4900 ug/g- TH*°*
<0.2 ug/1 .
<0.2 ug/1
11.8 ug/1. itV*
0.42 ug/1
<10 ug/g
<10 ug/g
68 ug/g
78 ug/g
DATA
PCB's
-
• •-
-
<0.5 ug/1*
-------
OUTLET OF PRECIPITATOR
TABLE
Test 110/2-14
POLLUTANT
SAMPLE NUMBER
Antimony
Arsenic
Barium
Beryllium
Cadmium
Calcium
Chromium
Cobalt
Copper
Iron
Lead
Manganese
Mercury
Nickel
Selenium
Tellurium
Tin
Titanium
Vanadium
Zinc
Chloride
Fluoride
Nitrates
Sulfates
M*
.003
o.lS
0.0?
/OSO
/.S
O. /
2.
2.0
/O
-------
OUTLET OF PKECIFITATOR
TABLE
Test 010/2-14
POLLUTANT
SAMPLE NUMBER
Antimony
Arsenic
Barium
Beryllium
Cadmium .
Calcium
Chromium
Cobalt
Copper
Iron
Lead
Manganese
Mercury
Nickel
Selenium
Tellurium
.Tin
Titanium
Vanadium
Zinc
Chloride
Fluoride
Nitrates
Sulfates
398+
(1*0
1100
10
Zoo
<2.000
0
<3«0
ST/000
396+
v>
<\
33
10
31.U
232,234
236,238
239
202,210 318,
211,313 319,
317 322
588
-------
TRACE SPECIES AND ORGANXCS TEST
SAMPLE RECOVERY LOG
Test No. lC^-|fe> Date 3/a/T/7(» location
Port Position QyTUET
Container
Number
Sanple Description
Container
Type
Net
wt/vol.
Comment
0.
11
44*
4-10.1
L*L
3
2S2.
W
JLM-
2*4
tl
.11
CsS
3V O
C2)
S2.I J
jLifciL
381
ttfc'tl
CM «•«•«•.
-72.1 J
450
Data Sheet KVB 6002-15
589
-------
TRACE SPECIES AND ORGANICS TEST
SAMPLE RECOVERY LOG
Test No.
Date
Location
Sample Port Position
Container
Number
Sample Description
Container
Type
Net
wt/vol.
Comment
Seuias. - tiw
4-1O
48. B
i\Z
zs.z
23
Is.fe
5S2.
to.l
100.0^
\oo.
• 2.1
4«>7J 49-2 if
(.0
ft)
\oiA-
l O.
\c».%
1— ^ Icjut) Moo
"P \ T^«
Data Sheet KVB 6002-15
590
-------
TEST 10/2-16 KVB ANALYSIS DATA
* J
Staple'No. . POM»i PCB'l
1 MI ' •.-; • "
582 . -
280 -
A'
267
294
Y
o'
li'
'i1:
1015
1014 '-'.,.
1.8 ug/1 < l,{
.9,810 ug/1- H**-
\ 582 ugy^A, $i«,W
0.26 ug/1
0.55 ug/1
<0.4 ug/1
<0.4 ug/L
<20 ug/g.
<20 ug/g,
<1 ug/1
-------
OUTLET OF PRECIPITATOR TABLE ' Test 110/2-16
POLLUTANT SAMPLE NUMBER
Antimony
Arsenic
-r
Barium .
Beryllium
Cadmium
Calcium
Chromium
Cobalt
Copper
Iron
Lead
Manganese
Mercury
Nickel
Selenium ~
Tellurium.
Tin
Titanium
Vanadium
Zinc
Chloride
Fluoride
Nitrates
Sulfztes
381+
<2.oo
—
2.00
— .
—
—
—
— •
tgSbb
OTO}
<\
—
00
CZ^o)
—
^o.oo3
^o.o,
/•3
^* / s
^o»oi*
oS
o.//
.S1
ra..^.
^W^^'^r
^^D 7a^^
2.S
294+
'S
2.0
/. s
Ho
10
z
—
os
0:
-------
OUTLET OF FRECIFITATOR TABLE Test 10/2-16
POLLUTANT SAMPLE NUMBER
Antimony
Arsenic
iarium
Beryllium
Cadmium
Calcium
Chromium
Cobalt
Copper
Iron
Lead
Manganese
Mercury
Nickel
Selenium
Tellurium
Tin
Titanium
Vanadium
Zinc
Chloride
Fluoride
Nitrates
Sul fates
B*
^f^^t^f •
^£o_$2J&
. —
3
o.ot
0* C»
o WM
o.os
O-ot.
2..0
<0./
o.on3
^IflB
t
<\o.<&
-------
COMMERCIAL TESTING & ENGINEERING CO.
•INI**!, orncui it* NORTH LA «*u.t trim, CMio»ao, ULINOII «eioi • A»IA oooi in MI-MM
Reply tO INtltUMINTAl ANAinil OIVIIION. I43U Will MTN AV1NUI, OOIOIN, COlOtAOO M«1, MONIi JOW7WSJ1
To: Mr. John G, Mlchalovlc ^l&.
Calspan Corporation —•«•
Post Office Box 235
Buffalo, NY 14221
P.O. No., 27810
Semple No.: 1Q/2 - 16
ELEMENT CONC.
Uranium <>.06
Thorium <0.08
Bismuth <0.02
Lead 0.05
Thallium
Mercury NR
Gold
Platinum
Ir1d1um
Osmium
Rhenium
Tungsten
Tantalum
Hafnium
Lutetlum
Ytterbium
Thulium
Erbium
Hoi ml urn
Dysprosium
NR ••• Not Reported
All element* not reported <
A Comp. 448, 226, 237,
CONCENTRATION
ELEMENT CONC.
Terbium
Gadolinium
Europium
Samarium
Neodymlum
Praseodymium
Cerium
Lanthanum
Barium 0.04
Cesium 0.003
Iodine March 8r 1977
Anelytti S. Sweeney
IAD NO.I
CONC.
0.07
0.03
0.04
0.02
0.08
<0.02
<0.004
<0.005
<0.007
0.1
0.03
0.04
0.007
0.5
0.1
*0.4
VM
97-A101-134-21
ELEMENT
Vanadium
Titanium
, Scandium
Calcium
Potassium
Chlorine
Sulfur
Phosphorus
Silicon
Aluminum
Magnesium
Sodium
. Fluorine
Oxygen
Nitrogen
Carbon
Boron
Beryllium
Lithium
Hydrogen
^K~^~&--i&L
CONC.
<0.002
0.04
-------
COMMERCIAL TESTING & ENGINEERING CO.
.OENEKAL OFFICE*: »• NORTH LA IALLE STKEIT, CHICAQO, ILLINOIS (0(01 • AlEA CODE 112 T9I-MI4
Reply to iNsmiMiNTAi ANALYSIS DIVISION. 14335 WEST «TH AVINUE. GOLDEN. COIOIADO KMOI. PHONE, 303-271-9331
To: Mr. John G. Michalovlc
Calspan Corporation
Post Office Box 235
• Buffalo. NY 14221
P.O. NO.I 27810
Sample No.: 10/2 . 16 B Con,p. 294 1/27/77
Date: March 81, 197
S. Sweeney
IAD No.: 97-A101-134-21
ELEMENT CONC.
Uranium
Thorium
Bismuth
Lead <2
Thallium
Mercury NR
Gold
Platinum
Irldlum
Osmium
Rhenium
Tungsten
Tantalum
Hafnium
Lutetium
Ytterbium
Thul 1 urn
Erbium
Hoi mi urn
Dysprosium
heterogeneous
NR - Not Reported
All elements not reported
Sample was thermally
CONCENTRATION
ELEMENT CONC.
Terbium
Gadolinium
Europium
Samarium
Neodymlum
Praseodymium
Cerium
Lanthanum
Barium 2
Cesium
Iodine
Tellurium
Antimony
Tin <.!
Indium STD
Cadmium
Silver
Palladium
Rhodium
-------
COMMERCIAL TESTING & ENGINEERING CO.
aENCHAt. OFFICE*: f »• HOVTH LA (AU.E STREET, CHICAGO, IU.INOII (0601 • A>EA CODE III T««-»4I4
Reply tO INSTtUMENTAl ANALYSIS DIVISION, I«HJ WEST 44TH AVENUE. COIOEN. COIORAOO KMDI. PHONEi JCO-I7WS3I
TO: Mr. John G. M1chalov1c
Calspan Corporation
Post Office Box 235
Buffalo, NY 14221
P.O. No.: 27810
Sample No.: 10/2 i6 c 1267, 325, 326, 327, 328, 329,
309! 310*. 312* CONCENTRATION IN
Date: March 11, 1977
Analyst-. S. Sweeney
IAD No.: 97-A101-134-21
ELEMENT CONC.
Uranium
Thorium
Bismuth
Lead . «>.03
Thallium
Mercury NR
Gold
Platinun
Iridium
Osmium
Rhenium
Tungsten
Tantalum
Hafnium
Lutetian
Ytterbium
Thulium
Erbium
Hoi mi urn
Dysprosium
ELEMENT
Terbium
Gadolinium
Europium
Samarium
Neodymium
Praseodymium
Cerium
Lanthanum
Barium
Cesium
Iodine
Tellurium
Antimony
Tin
Indium
Cadmium
Silver
Palladium
Rhodium
CONC.
0.01
0.01
0.04
0.06
0.004
0.009.
0.1
0.2
STD
<0.01
MC
ELEMENT
Ruthenium
Molybdenum
Niobium
Zirconium
Yttrium
Strontium
Rubidium
Bromi ne
Selenium
Arsenic
Germanium
Gallium
Zinc
Copper
Nickel
Cobalt
Iron
Manganese
Chromium
CONC.
0.04
0.03
0.01
<0.006
0.01
0.003
0.05
0.4
<0.004
0.02
0.5
0.08
0.1
0.006
0.8
0.08
0.3
ELEMENT
Vanadium
T1 tani urn
Scandium
Calcium
Potassium
Chlorine
Sulfur
Phosphorus
Silicon
Aluminum
Magnesium
Sodium
Fluorine
Oxygen
N1 trogen
Carbon
Boron
Beryllium
Lithium
Hydrogen
CONC.
0.02
<0.2
<0.009
MC
3
1
MC
3
*2
0.08
2
MC
«4
NR
NR .
NR
0.2
0.04
NR
NR - Not Reported
All elements not reported < 0.007 yg/nil
^Heterogeneous
Approved:
506
-------
COMMERCIAL TESTING & ENGINEERING CO.
Of NE»Al OrriCU: tt« MOUTH LA (ALIC tTREET, CHICAGO, ILLIHOK MtOt • A*IA COOi lit T8«-»4»4
Reply to iNsmiMiNTM ANAUM DIVISION. 14335 WIST MTM AVCNUE. OCHDCN. cmotAoo MUOI. rnoni, JOJ.JTMSI
TO! Mr. John 6. Mlchalovlc ^ML.
Cat span Corporation ~°~-
Post Office Box 235 Daf* March 8, 1977
Buffalo, NY 14221
Analyst: S. Sweeney
P. 0. No.: 27810
SompleNo.: 10/2 . 16 „ Conip0s1te 11014 1/27/77 IAD No-! 97-A101- 134-21
CONCENTRATION IN PPM WEIGHT
ELEMENT CONC.
Uranium <0.3
Thorium <0.4
Bismuth <0.1
Lead 0.4
Thallium
Mercury MR
Gold
Platinum
Irldlum
Osmium
Rhenium
Tungsten
Tantalum
Hafnium
Lutetlum
Ytterbium
Thulium
Erbium
Hoi ml urn
Dysprosium
NR - Not Reported
All AlAm*nf* nnf HtrvurftjwJ ,
ELEMENT
Terbium
Gadolinium
Europium
Samarium
Neodymlum
Praseodyml urn
Cerium
, Lanthanum
Barium
Cesium
Iodine
Tellurium
Antimony
Tin
Indium
Cadmium
Silver
Palladium
Rhodium
***A 1 *inm t*s*lMk»
CONC.
<0.1
0.1
0.1
0.3
0.1
0.1
0.2
0.5
52
0.3
1
0.2
<0.1
STD
<0.1
ELEMENT
Ruthenium
Molybdenum
Niobium
Zirconium
Yttrium
Strontium
Rubidium
Bromine
Selenium
Arsenic
Germanium
Gallium
Zinc
Copper
Nickel
Cobalt
Iron
Manganese
Chromium
<600
MC
>300
560
330
>49
450
>150 ;
«68
NR
NR
NR
15
<0.1
>140
. NR
^
Sample was thermally ashed 9 350° C for
crucible Prior to analysis.
one hour 1n a laboratory furnace 1n a quartz
597
-------
COMMERCIAL TESTING & ENGINEERING CO.
OENEIAL OFFICE*: ttt NORTH LA IALLE STREET. CHICAGO, ILLINOIS (0(01 • AREA CODE (13 7>t-t4»4
Reply to iNsnuwNTAL ANALYSIS DIVISION. iati WEST UTH AVENUE. GOLDEN. COLWADO KMOI, PHONE:
To: Mr. John G. M1chalov1c
Calspan Corporation
Post Office Box 235
Buffalo. NY 14221
Date: March 9, 1977
P.O. No.: 27810
Sample No.: 1Q/2 jg
ELEMENT CONC.
Uranium <1
Thorium <2
Bismuth <0.4
Lead <0.8
Thallium
Mercury NR
Gold
Platinum
Ir1d1um
Osmium
Rhenium
Tungsten
Tantalum
Hafnium
Lutetlum
Ytterbium
Thulium
Erbium
Hoi ml urn
Dysprosium
E Comp. #1013 1/27/77
CONCENTRATION
ELEMENT CONC.
Terbium
Gadolinium
Europium
Samarium
Neodymium
Praseodymium
Cerium 0.2
Lanthanum 0.5
Barium 9
Cesium 0.2
Iodine 2
Tellurium
Antimony
Tin fO.4
Indium STD
Cadmium
Silver
Palladium
Rhodium
IN PPM WEIGHT
ELEMENT
Ruthenium
Molybdenum
Niobium
Zirconium
Yttrium
Strontium
Rubidium
Bromine
Selenium
Arsenic
Germanium
Gallium
21 nc
Copper
Nickel
Cobalt
Iron
Manganese
Chromium
Analyst:
IAD No.:
CONC.
0.8
<0.1
2
33
4
<0.7
3
0.6
10
2
2
0.1
37
210
0.1
S. Sweeney
97-A101-134-21
ELEMENT
Vanadium
Titanium
Scandium
Calcium
Potassium
Chlorine
Sulfur
Phosphorus
Silicon
Aluminum
Magnesium
Sodium
Fluorine
Oxygen
Nitrogen
Carbon
Boron
Beryllium
Lithium
Hydrogen
CONC.
0.3
22
<2
430
MC
MC
MC
650
260
6
170
MC
-67
NR
NR
NR
24
18
NR
NR - Not Reported
All elements not reported <0.2ppm weight
Approved:
598
-------
CARBON MONOXIDE BOILER
Location No. Unit No
Unit Description
CO G» A*6 t^o t FL.O \T> CctAi_y-r id- CE-A^V! i t^a O
(PCCO)R
oool k
Installation Date
Heater Rating
Burner Description 4" "E; '^ ^^"P "WPS-
Test Fuel Combinations
Fuel Temp, at Burner (°F)
Primary Air Temp. (°F) 7^^ K
Comments:
-------
Test No
.11-'
Date
MOBILE LABORATORY DATA
Location_JJ_
C.O +
Test No.M "~ I
Engr.
Unit No.
Capacity
Unit Type
Burner Type
Sp»d <£«*> & K,
1. Test No.
2. Date
3. Time
4. Load Klb *&«M //»<"
5. Process Rate
6. Flue Diam. or Size, ft
7. Probe Position
8. Oxygen (%)
9. NOx (hot) read/3% 02 (ppm)
10. NO (hot) read/3% 02 (ppm)
11. NO? (hot) read/3% 02 (ppm)
12. NO (cold) read/3% O2 (ppm)
13. Carbon Dioxide (%)
14. Carbon Monoxide (ppm) uncor/cor
15. Hydrocarbon (ppm) uncor/cor
16. Sulfur Dioxide (ppm) uncor/cor
17. Smoke Spot (Bacharach)
18. Atmos. Temp. (°F/*I&)
19. Dew Point Temp. (°F/\)
20. Atmos. Pressure (in. Hg)
21. Relative Humidity (%)
22.
23.
24.
25.
26.
27.
28.
29.
30.
U- 1
l-l-lt.
n+yo
2^2.
CD
z.«
\\o
no
o
mo
(3,
2VJ
\9
1(fO
•M
>
lD*f
Io4
0
/i3
<^
Z."^)
<;•
720
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600
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Test No. 1 1-*Z-
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MOBILE LABORATORY DATA
Date3-*7-"7Cg Location _ |J_
Test No. I I -7.
Engr.
Fuel£*f. &» & Capacity
Onit Type CQ
Burner Type_
1. Test No.
2. Date
3. Time
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5. Process Rate
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7. Probe Position
8. Oxygen (%)
9. NOx (hot) read/3% 02 (ppm)
10. NO (hot) read/3% 02 (ppm)
11. NO? (hot) read/3% 02 (ppm)
12. NO (cold) read/3% O2 (ppm)
13. Carbon Dioxide (%)
14. Carbon Monoxide (ppm) uncor/cor
15. Hydrocarbon (ppm) uncor/cor
16. Sulfur Dioxide (ppm) uncor/cor
17. Smoke Spot (Bacharach)
16. Atmos. Temp. ("F/*^
19. Dew Point Temp. (DF/°>M
20. Atmos. Pressure (in. Hg)
21. Relative Humidity (%)
22.
23.
24.
25.
26.
27.
28.
29.
30.
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Data Sheet 6002-2
60
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Test No. I i- "3
Unit No. 2.
MOBILE LABORATORY DATA
Pate ^~%-7£ Location, IJ_
•£3^
Puelgf-r. ftff^ Capacity
Test
Engr.
Onit Type CO
Burner Type
1. Test No.
2. Date
3. Time
. ., 1 1 . i / ,
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5. Process Rate
6. Flue Diam. or Size, ft
7. Probe Position
a. Oxygen (%)
9. NOx (hot) read/3% 02 (ppm)
10. NO (hot) read/3% 02 (ppm)
11. NO? (hot) read/3% 02 (ppm)
12. NO (cold) read/3% 02 (ppm)
13. Carbon Dioxide (%)
14. Carbon Monoxide (ppm) uncor/cor
15. Hydrocarbon (ppm) uncor/cor
16. Sulfur Dioxide (ppm) uncor/cor
17. Smoke Spot (Bacharach)
v
16. Atmos. Temp. (°P/*V)
v
19. Dew Point Temp. <°F/°aj
20. Atmos. Pressure (in. Hg)
21. Relative Humidity (%)
22.
23.
24.
25.
26.
27.
28.
29.
30.
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602
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MOBILE LABORATORY DATA
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unit Type
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10. NO (hot) read/3% 02 (ppm)
11. NO? (hot) read/3% 02 (ppm)
12. NO (cold) read/3% 02 (PPm)
13. Carbon Dioxide (%)
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15. Hydrocarbon (ppm) uncor/cor
16. Sulfur Dioxide (ppm) uncor/cor
17. Smoke Spot (Bacharach)
18. Atmos. Temp. ("F/^O
19. Dew Point Temp. (0F/"C)
20. Atmos. Pressure (in. Kg)
21. Relative Humidity (%)
22.
23.
24.
25.
26.
27.
28.
29.
30.
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603
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Test Ho. I'" 5
Unit Ho. "2-
MOBILE LABORATORY DATA
Date +•
Fuel ggA6g3 Capacity
Test Ho.i
unit Type
Burner Type
1. Test No.
2. Date
3. Time
4. Load ^ 'b S7»4rv\.//VK-
5. Process Rate
6. Flue Diam. or Size, ft
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8. Oxygen (%)
9. NOx (hot) read/3% 02 (ppm)
10. HO (hot) read/3% 02 (ppm)
11. NO? (hot) read/3% 02 (PPm)
12. NO (cold) read/3% 03 (ppm)
13. Carbon Dioxide (%)
14. Carbon Monoxide (ppm) uncor/cor
15. Hydrocarbon (ppm) uncor/cor
16. Sulfur Dioxide (ppm) uncor/cor
17. Smoke Spot (Bacharach)
18. Atnos. Temp. (°F/*X)
19. Dew Point Temp. (°F/*|R)
20. Atmos. Pressure (in. Hg)
21. Relative Humidity (%)
22.
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24.
25.
36.
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MOBILE LABORATORY DATA
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Capacity
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3. Time
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6. Flue Diam. or Size, ft
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8. Oxygen (%)
9. NOx (hot) read/3% 02 (ppa)
10. NO (hot) read/3% 02 (ppm)
11. NO? (hot) read/3% 02 (ppm)
12. NO (cold) read/3% 02 (ppm)
13. Carbon Dioxide (%)
14. Carbon Monoxide (ppm) uncor/cor
15. Hydrocarbon (ppm) uncor/cor
16. Sulfur Dioxide (ppm) uncor/cor
17. Smoke Spot (Bacharach)
18. Atmos. Temp. (°F/*i£)
19. Dew Point Temp. (°F/^l£)
20. Atmos. Pressure (in. Hg)
21. Relative Humidity (%)
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6 05
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Test Ho. — *?
MOBILE LABORATORY DATA
Date 2»oi
Burner Type
B«fH/ Sy>
1. Test Vo.
2. Date
3. Time
4. Load ^ '& S'fedM/kv*"
5. Process Rate
6. Flue Diam. or Size, ft
7. Probe Position
8. Oxygen (%)
9. NOx (hot) read/3% 02 (ppm)
10. NO (hot) read/3% 02 (ppm)
11. NO? (hot) read/3% 02 (Ppm)
12. NO (cold) read/3% 02 (ppm)
13. Carbon Dioxide (%)
14. Carbon Monoxide (ppm) uncor/cor
15. Hydrocarbon (ppm) uncor/cor
16. Sulfur Dioxide (ppm) uncor/cor
17. Smoke Spot (Bacharach)
18^ Atnos. Temp. (°F/«c)
19. Dew Point Temp. (eF/°C)
20. Atmos. Pressure (in. Bg)
21. Relative Humidity (%)
22.
23.
24.
25.
26.
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606
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Test No._
Obit No.
MOBILE LABORATORY DATA
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607
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MOBILE LABORATORY DATA
Location / '
Capacity
Teat Mo.
Engr. Woo
Burner Type
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2. D»te
3. Time
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9. NOx (hot) read/3% 02 (ppm)
10. NO (hot) read/3% 02 (PPO)
11. N05 (hot) read/3% 02 (ppm)
12. NO (cold) read/3% 02 (ppm)
13. Carbon Dioxide (%)
L4. Carbon Monoxide (ppm) uncor/cor
15. Hydrocarbon (ppm) uncor/cor
16. Sulfur Dioxide (ppm) uncor/cor
17. Smoke Spot (Bacharach)
18. Atmos. Temp. (•F/'-QJ
19. Dew Point Temp. ("F/"^
20. Atmos. Pressure (in. Hg)
21. Relative Humidity (%)
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Data Sheet 6002-2
608
-------
OPERATING DATA
Location 11
FCCU CO BOILER
Sheet 1 of 2
Test No.
Date
Time
Test Typ^f
Burner out of Service
Bl AR Position, notches open*
B2
B3
B4
NO Ports, leftside, % open
NO.. Ports, right side, % open
Steam Flow (lbs/hr x 40,000)
Steam Drum Pressure (psig)
Steam Header Pressure (psig)
Feedwater Flow (lbs/hr x 40,000)
Boiler Slowdown (lbs/hr x 6,000)
Fuel Gas Flow (SCF)| x 50,000)
Combustion Air (lbs/hr x 40,000)
Fuel Gas Header Pressure (psig)
Fuel Gas Burner Pressure (psig)
Pilot Gas Pressure (psig)
F.D. Fan Discharge (in.)
Hindbox Pressure (in.)
CO Duct Pressure (in. )
Furnace Pressure (in.)
Economizer Inlet Pressure (in.)
Economizer Outlet Pressure (in.)
BFW Pump Discharge Pressure (psig)
DeA FW Pump Pressure (psig)
Stack Opacity
Flue Gas O_, % (Control Boon)
Combustibles, %
//-/
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OPERATING DATA
Location 11
FCCO 00
Sheet 2 of 2
Test Mo.
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Economizer Cas Inlet (*F)
950
Economizer Gas Outlet (*F)
sso
560
S6S
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Economizer Water Inlet (*F)
7,50
Economizer Water Outlet (*F)
4SO
Ahead of Gen. Bank (*F)
Flue Gas Exit (*F)
CO Ca* Inlet («F)
^2.5
Statun-Dxuir. Steao Out ("F)
SZS
Furnace Tamperatur* (*F)
1140
• •7-75
nwo
Barometric Pressure (in. Ho)
88
Relative Humidity (%)
60
Ambient Temperature (*F)
RE08NERATOR DATA
Lift Air Flow (Itos/hr)
Combustion Air Flow (Ibs/hr)
Cyclone Steam (Ibs/hr)
isto
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Cyclone Water (OFM)
flpray Water (0PM)
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61 0
-------
OPERATING DATA
Location 11.
FCCU CO BOILER
Sheet 1 of 2
Test No.
Date
Time
Test Type-
Burner out of Service
Bl AR Position, notches open*
B2
B3
B4
NO Ports, leftside, % open
NO Ports, right side, % open
Steam Flow (Ibs/hr x 40.000)
Steam Drum Pressure (psiq)
Steam 'Header Pressure (psiq)
Feedwater Flow (Ibs/hr x 40,000)
Boiler Slowdown (Ibs/hr x 6,000)
Fuel Gas Flow (SCFN x 50,000)
Combustion Air (Ibs/hr x 40,000)
Fuel Gas Header Pressure (psig)
Fuel Gas Burner Pressure (psig)
Pilot Gas Pressure (psiq) •
F.b. Fan Discharge (in.)
Windbox Pressure (in.)
CO Duct Pressure (in.)
Furnace Pressure (in.)
Economizer Inlet Pressure (in.)
Economizer Outlet Pressure (in.)
BFW Pump Bischarge Pressure (psig)
DeA FH Pump Pressure (psiq)
Stack Opacity
Flue Gas O_, % (Control Room)
Combustibles, %
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OPERATING DATA
Location 11
FCCU CO BOILER
Test No.
Date
Time
SH Steam'Out (*F)
DeSH Steam Out (°F)
Economizer Gas Inlet (°F)
Economizer Gas Outlet (°F)
Economizer Hater Inlet (°F)
Economizer Hater Outlet (°F)
Ahead of Gen. Bank (°F)
Flue Gas Exit (°F)
CO Gas Inlet (°P)
Steam Drum Steam Out (°F)
Furnace Temperature (*F)
Barometric Pressure (in. Hg)
Relative Humidity (%)
Ambient Temperature (°F)
REGENERATOR DATA
Lift Air Flow^ (Ibs/hr)
Combustion Air Flow (Ibs/hr)
Cyclone Steam (Ibs/hr)
Cyclone Hater!' (GPM)
Spray Hater (GPM)
Comments «
li-(p
^•^-76.
I/CO
noo
5
l<4lO
t C&^^
(ooQ
IIS
555
"Z6>O
MSO
1435
ESS
^ZS
SS5
/&7S
—
—
• —
iis%»a
1 -W woo
*7^0O
0
O
HOj, fttfT*
itrr net
CO GAS-*-
IKS
47-c}-7^3
/uso
1OO
S«?S
- f Z5
sso
ZSS
ISO
/wzo
^3 £r~^\
Q^y^^ '
«?2o
S30
/6S5
—
—
'—
)ZS3^
OS^eo
£4OO
0
O
IK*?
-------
OPERATING DATA
Location 11
FOCD CO BOILER
Sheet 1 of 2
Test No.
Date
Time '
Test Type*
Burner out of Service
Bl AR Position, notches open*
B2
B3
B4
NO Ports, leftside, % open
NO Ports, rightside, % open
Steam Flow (Ibs/hr x 40,000)
Steam Drum Pressure (psig)
Steam Header Pressure (psig)
Feedwater Flow (Ibs/hr x 40,000)
Boiler Slowdown (Ibs/hr x 6,000)
Fuel Gas Flow (SCFM x 50,000)
Combustion Air (Ibs/hr x 40,000)
Fuel Gas Header Pressure (psiq)
Fuel Gas Burner Pressure (psig)
Pilot Gas Pressure (psig)
F.D. Fan Discharge (in.)
Windbox Pressure (in.)
CO Duct Pressure (in.)
Furnace Pressure (in.)
Economizer Inlet Pressure (in.)
Economizer Outlet Pressure (in.)
BFW Pump Discharge Pressure . (psig)
•DeA FM Pump Pressure (psig)
Stack Opacity
Flue Gas 0, , % (Control Room)
Combustibles, %
ll-ll
q-io-ib
01 SO
tf>/S
ttz
• "b
/•*>
l(f
/6>
o
o
"1,0
(elS
S^S
•7,0
?./
4.0
s.s
<-*s
^5
10+
is.-z.
I2.O
12,5
J^.S
5
o.o
W(*
=»r
•L^
2..W5
O
I)~l1
l-ib-tf?
12,^0
o/s
*<+
13
13
1C,
1(0
o
o •
•7.J
(oTi.
S^4
-?./
<£,(*
4.0
?,(b
^5
^,5
.0^
is,9
/z,g
IS
13
S,^
O .O
3M&
*r
1A
t >0
O
lh>3
<*-it>--)^>
l^Zo
B^^^voe
fJo»*.
IB
'i
\<0
\(c
O
O
6.9S
673
S9«/
-7.1
?,&
4.o
8,7
46
2,S
Iff*
»S, ....
2,S
O
1
..-,--. .
,
• 19 notches is full open
6 1 3
-------
OPERATING DATA
Location 11
FCCU CO BOILER
Sheet 2 of 2
Test No.
Date
Time
SH Steam .Out (°F)
DeSH Steam Out (°F)
Economizer Gas Inlet (°F)
Economizer Gas Outlet (°F)
Economizer Hater Inlet (°F)
Economizer Water Outlet (°F)
Ahead of Gen. Bank (°F)
Flue Gas Exit (eF)
CO Gas Inlet (°F)
Steam Drum Steam Out (°F)
Furnace Temperature (°F)
Barometric Pressure (in. Hg)
Relative Humidity (%)
Ambient Temperature (°F)
REGENERATOR DATA
Lift Air Flow (Ibs/hr)
Combustion Air Flow (Ibs/hr)
Cyclone Steam (Ibs/hr)
Cyclone Water (GPM)
Spray Water (GPM)
IM/
3-10-1(0
<3«T 50
1OO
£05
310
520
Zj(oo
4So
\<-too
ZHO
*no
5?>0
1&U5
—
—
—
(Z53.33
< SS Soo
T7OO
O
O
11-11
9-jo--?4>
/Z50
-70O
5^?5
90S
s«/e»
z^o
ft|5
/V3o
?SO
°ito
S2.Q
\(oSO
—
—
—
ICeOtcaci
•7-7oo
O
O
//-'?
«?-/£> --?6
^3.2.0
•7OO
SfS
loo
S2.5
Z^O
W5
/wo
8^5
^/oo
•7-70O
O
O
1
'
'•
.
:
'•
I
Comments:
f
t.ffr nee
CO GAS-
(*/
<*__•'
"N
*3\
OK POKTS,
RI6HT
6 1 4
-------
run, MOUYIU
T..t *>
I/-/
Chit
Location
•oar
Bacfle Point.
rtMl
*y.
2fi£
CB4 Methane
C.H. Bthane
CIHI Propane
eyf Butane
OCr Pentane
Bthylene
Propylene
Butylene
Pentylene
Acetylene
Bencene
Ol " Oxygen
III Nitrogen
00. carb. Oiox
CO* carb. Nonox
• cr air Btu(HHV) or coa cr mo cr prod
Voluna CT fuel CT fuel Cf fuel Cf fuel CT fuel
.^•^^•^••MV
0.0955
0.1671
0.2387
0.3103
0.3619
0.1432
0.2148
0.2669
0.3580
0.1193
0.3580
-0.0477
9.94
17.51
25.19
33.21
41.11
15,80
23.33
31.23
39.16
14.57
36.46
0.0239
0.0239
3.15
3.18
0.01
0.02
0.03
0.04
0.05
0.02
0.03
0.04
0.05
0.02
0.06
0.01
0.01
0.02
0.03
0.04
0.05
0.06
0.02
0.03
0.04
0.05
0.01
0.03
0.01
0.1055
oaeai
.2587
.3353
.4119
.1532
.2298
.3068
.3830
.1343
.3730
.0377
.01
.01
.0289 <
.0289 (
.000416
.000786
.001171
.001548
.001864
.000726
.001087
.001449
.001813
.000682
D.002017
.000828
.000728
.001145
).000724
). 0000522
Total IQOiQ
Theoretical Airi
•crair . era
10* Btu CT fuel
8CT air CT air ,-6 /
* 40 /
Btu 0 7o*r,
29.92 in. Bg.
ttu
Ml X (08CT/106 Mtt)
K' • 3^430
lto/10* JKU - (ppm 6 3* 03)/K
3»
6003-6 (Rav. 1)
61 5
-------
Test No 11- I
Unit No. 1
Date
GASEOUS FUEL ANALYSIS
// -
Location
Test Mo J*~/
Bngr
Fuel Sample No_
Fuel Sample Point
Fuel Analysis by
Gas
CH4
C2H6
£{
C2H4
c4
Sf
(XT
% CF air Btu(HHV) CF CO2 CF KyO CF Prod Ib Prod
Volume CF fuel CF fuel CF fuel CF fuel CF fuel CF fuel
Methane
Ethane
Propane
Butane
Pentane
Ethylene
Propylene
Butylene
Pentylene
Acetylene
Benzene
Oxygen
Nitrogen
Garb. Diox
Carb. Monox
Hydrogen
x 0.0955
x 0.1671
0.2387
0.3103
0.3819
0.1432
0.2148
0.2869
0.3580
0.1193
0.3580
x -0.0477
x 0.0239
x 0.0239
9.94
17.51
25.19
33.21
41.11
15.80
23.33
31.23
39.16
14.57
38.48
3.15
3.18
0.01
0.02
0.03
0.04
0.05
0.02
0.03
0.04
0.05
0.02
0.06
0.01
0.01
0.02
0.03
0.04
0.05
0.06
0.02
0.03
0.04
0.05
0.01
0.03
0.01
0.1055
0.1821
0.2587
0.3353
0.4119
0.1532
0.2298
0.3068
0.3830
0.1343
0.3730
-0.0377
o.oi
0.01
0.0289
6.0289
0.000416
0.000786
0.001171
0.001548
0.001864
0.000726
0.001087
0.001449
0.001813
0.000682
0.002017
0.000828
0.000728
0.001145
0.000724
0.0000522
Total
Theoretical Air:
SCF air CF air
KSCF Prod
106 Btu
% Moisture -
DSCF Prod
106 Btu
% O>2, dry
K _ " 331.5xl06
100,0
1 0.6
-------
GASEOUS FUEL ANALYSIS
Test NO 1 1- /
Date ^
Unit No. "Z. Fuel^
Fuel Sample Point Rf^fWetl
Gas
CH4
C2H6
C3H0
C H
C!JH"
C»H*
CAHR
C*H
C2H2
ob fc
»:
c60
CO*
H2
Methane
Ethane
Propane
Butane
Pentane
Ethylene
Propylene
Butylene
Pentylene
Acetylene
Benzene
Oxygen
Nitrogen"*
Carb. Diox
Carb. Monox
Hydrogen
Ototal
^
%
Volume
x
x
X
X
X
X
. . x
X
X
X
X
O.fi x
ffiPiO
<*.<4
*X x
X
\OO,O <
Test No ' '" '
-1-~1{p Location '/
5£*?S
Engr
Fuel Sample No
D/* 0«f /.«t Fuel Analysis by
CF air
CF fuel
0.0955
0.1671
0.2387
0.3103
0.3819
0.1432
0.2148
0.2869
0.3580
0.1193
0. 3580
-0.0477
0.0239
0.0239
Btu(HHV)
CF fuel
9
17
25
33
41
15
23
31
39
14
38
3
3
.94
.51
.19
.21
.11
.80
.33
.23
.16
.57
.48
.15
.18
CF CO2
CF fuel
0.01
0.02
0.03
0.04
0.05
0.02
0.03
0.04
0.05
0.02
0.06
0.01
0.01
u
rft
CF H?0
CF
0
0
0
0
0
0
0
0
0
0
0
0
fuel
.02
.03
.04
.05
.06
.02
.03
.04
.05
.01
.03
.01
0v
CF
CF
0
0
0
0
0
0
0
0
0
0
0
-0
0
0
0
0
tiPiBV'
Prod
fuel
.1055
.1821
.2587
.3353
.4119
.1532
.2298
.3068
.3830
.1343
.3730
.0377
.01
.01
.0289
.0289
«•
Ib Prod
CF fuel
0.000416
0.000786
0.001171
0.001548
0.001864
0.000726
0.001087
0.001449
0.001813
p. 000682
0.002017
0.000828
0.000728
0.001145
0.000724
0.0000522
Q-l^l ^&< 9 0I/9Z O '''W~7/ O.O768
Theoretical Air:
SCP air . <* air
10*> Btu CF fuel
WSCP Prod
IO6 Btu
CF Prod
CF fuel
6 / Btu(HHV) _
/ CF fuel
'1°6/5UfSl> "
*'*
SCF air/10 Btu 8 70"F,
29.92 in. Hg.
Net SCF Prod/106 Btu
% Moisture -
DSCF Prod
106 Btu
CF fuel
HSCF Prod
106 Btu
%H20
(100 -> Moisture)
Dry SCF/10 Btu
% C02, dry - i|
MW x (DSCF/106 Btu)
K* -K/-430
lb/106 Btu - (ppm e 3t 02)/K
ng/J «
3% O2>/K'
Data Sheet 6002-6 (Rev. 1)
6 1 7
-------
Met
Oait
PARTICULATE EMISSION CALCUIATIOM
Location / /
Puelg«£.
Sarelinq Train and Method
Fitot factor, Pe
lot. liquid Collected, V
O
Velocity Bead, AP O.lftd • »«
• «•
*R Stack Ar«a, A»
ft
Voluae, V»J4).) ft3 stack Preee., Peotd • 0.0474 VJc
3. Moieture Content BUD • Cq. 2/(Eq, 1 + Cq. 2)
4. Concentration a. C • 0.0154 Mn/Va ...
eta
b. C - 2.205 x 10~6 Mn/Va
c. C - Cq. 4b x 16.018 x 10
5. Abe. Stack Preee. Pe - Pfe)|y x 13.6 + Peg
6. Stack Cat speed Ve - 174 Pe I®?* , x
£&.
407
7. Stack Oae Plow a. Qew - Cq. 6 x As x
Bate • 70*P
b. fied - xq. 7a x (l. - sq> 3)
8. Material Flow Me - Eq. 7b x Eq. 4b x 60
9. *t>2 factor »2f - 2090/(20.9 - »2*)
10. Caieeion a. I • Bq. 4b x Pe x Cq. 9
b. S • Iq. 4c x Pa x Cq. 9 x 1000
11. » Xeokinetio
14077 x
Z -
0 x Ve x Pe x
Pe SC Peet/104 Btn
fh SC Mctere/104 joulee
Oil .
92.2
0.002475
Gae
07.4
0.002346
Coal
98.2
0.002636
,6CF
N.D.
, oraine/DSCP
*K> araae/DSCM
in. „ .be.
8^ S5
M8CF/«in
pscp/ain
Ib/hr
\tO.(o M.D.
Ib/MHStu
• '00Z3M6
ag/jonle
•Multiply
by 530/»('IO if awt«r not
'. eoopeneated.
Data Sbaet 6002-4
618
-------
Test Ho.
unit Ho.
Date
PARTICTLATE EMISSION CALCULATIONS
Location /
Fuel K*f. 64 i Sampling Train and Method Modi-Pitj >A
Pitot Factor, Fs
Barometric Pressure, P
Tot. Liquid Collected
ted, V^tn
.7.> of Sd*./i»
bar
ml Total Particulate,
n. Hg
m gm
.. o d*.pi»A s 012
Velocity Head, AP 0 .|&? o.'jaiwg Cfetack Temp. , Ts I O6O *R Stack Area, As JJ 3i I ft
Sample Volume, Vm U I ' / ft3 Stack Press., Pag O . / S> iwg Excess 02> «>a% 2 . Q' %
Orifice Press. Dif f . , H > iT.*? S iwg Stack Gas Sp. Gravity, Gg /
n.d.
Sample Tine, 6 tf5 mi" Nozzle Dia., Dn
*1. Sample Gas Volume
2. Water Vapor
_in. Meter Temp., T_ ~
• 0.0334 Vm(Pbar + H/13.6)
Vw . . - 0.0474 V,
sta ic
3. Moisture Content Bwo • Eq. 2/(Eq. 1 + Eq. 2)
4. Concentration a; C • 0.0154 Mn/Vm
std
•b. C - 2.205 x 10"6 Mn/Vm
c. C - Eq. 4b X 16.018 x 10
std
3
5. Abs. Stack Press. Ps - Px 13.6 + Psg
6. Stack Gas Speed : Vs - 174 Fs SteTa j- x g
7. Stack Gas Flow a. Qsw - Eq. 6 x As x |^ x ff=-
Rate 0 70eF Ts *07
• if. Qsd <• Eq. 7a x (1. - Eq. 3)
8.' 'Material Flow Ms • Eq. 7b x Eq. 4b x 60
9. XO. factor
10. Emission
11. % Zsokinetic
*>2f - 2090/(20.9 - K>2%)
a. E " Eq. 4b x Fe x Eq. 9
b. E - Eq. 4c x Fm x Eq. 9 x 1000
14077 X Ts(Vm + Vw )
6 x Vs x Ps x On2
Fe SC Feet/104 Btu
Fm SC Meters/104 joules
Oil
92.2
0.002475
Gas
87.4
0.002346
Coal
98.2
0.002636
5.93
SCF
SCF
N.D.
grains/DSCF
Ib/DSCF
grams/DSCM
in., w abs.
ft/min
WSCF/min
DSCF/min
Ib/hr
N.D.
Ib/MMBtu
•Multiply Vm .. by 530/T («R) if meter not temp, compensated.
•ta m
Data Sheet 6002-4
6 19
-------
Test No._
Box No.
PARTICULATE CALCULATION SHEET
!/- 3 Date ^'8-76 Location //
I Sample Probe Position
Test Description
Test Crew
Dry Gas Meter Vol.
Final
Initial
Total
(ft3)
^550.2,5"
41.IO
Final
Initial
A Vol
Inpinger Water Vol (ml)
100
/ oo
IOQ
S.
Total
Beaker No.
Filter
No.
I
Blank
No. 4
Date
Weighed
Tare
Wt.
I
, *, 7/1.1.
1-SJS57
6 loo
AW
Bottle No. <
Content I
Inpinger
(Water) fir
Probe
(Acetone)
Probe
(Water)
ZCO
Rinse (ml)
Date Weighed
or 250 Bake
-^
IOO.I2.IS
Final (1
Wt. 25072 \QO.IZ.
I LT I00.
1 Ol.oooo
Residue wt ^ =•/• t
Final 250-Tarefr»t.oni
.02,33
-,OOO2
Date Weighed
or 650 Bake
Final 1_
Wt. 650 2
Avg
Residue Wt
Final 650-Tare
Commentss
Data Sheet 6002-3
620
-------
PLANT
LOCATION //
OPERATOR
DATE ./lT
Stack .
Tempera-i
ture
(Ts) »F
600
&OO
&OO
6^0
6^>^
Velocity
Head
(P.)
7W, >4LO
e,3
-
- -
—
.. .
Pressure
Differen-
tial Acrot
Orifice
Meter
(AH),
In. H-O
/.S
/.z
1.1.
I.Z
s Gas
Sample
Volume
(Vm) ft3
ssso.zs
SS&i.oo
SSTT.OO
SS«J •,!»&
Gas Sample
Temperature at
Dry Gas Meter
^Snlet
(TmV\
nil. IV. I
°P^v
Outlet
(Tmout>
«p
?S
<=iS
IDS
HO
AVG.
AVG.
Sample
Box
remprta-
ture
•P
1ZO
3eo
230
3^0
AVR.
Temperature
of Gas
Leaving
Condenser on
>st Impinger
•P
&0
•7S-
•7S
•7S
CD
-------
Date
K V B. INC.
Test Ho. II—
SOx DATA SHEET
CO
TEST NOJ<"^ UNIT NO.7. FUEUg.4. LOAD I'M klb/hr
location
Box Mo.
Time
Temp, in Gas Meter
Press, in Gas Meter
Meter Reading
Barom. Press.
Percent Oxygen
1*2 Purge Time
O(p
\?>-LD
I0T-
O
•5,^0
^>o.o^>
.^'l
»S2S
O(o
)VS7
' <*(,
O
S.zso
"ao.o**,
•2..0
is4s
(A - B) x N x F x (460 + T) x 24
Excess o? 2^9 %
so2 -
A » Ml of lead perchlorate used for sample « ^ • i"*>
B = Ml of lead perchlorate used for bland = S,o
N » Normality of lead perchlorate titrant * >€>! (e~i
P » Barometric pressure •= "bO-0^
p - Pressure in gas meter - O
Concentration ,C, ppm m '_....
,gm/dscm •
. . Emission -,E, g/Mcal «
E » Cn 2090 I . Ib/MBtu "
where L •* ng/J -
C • pollutant concentration, g/dsen
Fr • volume factor - dscm/10 cal
dvcf/lQ4 fk£U
from Fed. Reg. 9/11/74 p 32856
so3
"2U. /
s,o
.x
1/2/75
622
-------
KVB, INC.
BOX DATA SHEET
TEST NO.l
OMIT MO/L
LOADJg)jL_iab/hr location / /
BOX MO.
Time
Tem$. in Gas Meter
Press, in Gas Mater
Meter Reading
Barom. Press.
Percent Oxygen
»2 'Purge Tine
tf>6»
mo6
I0T-
o
<^Z
afr
I **$. Ml of lead perchlorate used for sample -
B - Ml of lead perchlorate used for bland -
M • Normality of lead perchlorate titrant •
F » Dilution factor
T « Average.temp, in gas meter
V - Volume of gas sample ft3
P * Barometric pressure
p • Pressure in gas meter
Concentration ,C, ppa
8.
m /ZS
E* caf_ay°._1
bo.y-i.0j 1
«her*>- J
, g/Meal •
Ib/MBtu "
n«/J -
so
,0/46
2,8*5
C « pollutant concentration, g/dsea .
F, volume factor • dtca/10 cal
dsef/lO*
fr» Fed. teg. 9/11/74 p 12856
60-14
1/2/73
623
-------
PETROLEUM PROCESS HEATER
Location No . • \ i- Unit No. 1
Unit Description "PeT^pL€.UM
Comments:
Installation Date
Heater Rating
Burner Description
1913
2-7.5 vA'O
CO£M
f94->
DAZ
ao^'&^Ar^)
-S3, •
/
Test Fuel Combinations \\£,
"RE
F»k^E.(2.V G/s.«*
P'HSk\£^\
.1 £,AA i Ko. G 0,i_ 6-^^ SUM
T
Fuel Temp, at Burner
Primary Air Temp. (°
/Oi7\ >/ /
v ^ y /[/^ 0 > <&
F) x3^O
<*•// "^
^7&.5
^^ ^/r
,-^
624
-------
Test No. l2-/t-f_
Unit Ho. >
MOBILE LABORATORY DATA
-7< Location - 1
Test Mo.
Engr.
Fuel**/:
Capacity f7 * I0
Unit Type V£Xri£Al PXt>C£sS d£4r£& Burner Type
1. Test No.
2. Date
3. Time
4. Load
5. Process Rate
6. Flue Diam. or Size, ft
7. Probe Position
6. Oxygen (%)
9. NOx (hot) read/3% 02 (ppm)
10. NO (hot) read/3% 02 (ppm)
11. NO? (hot) read/3% 02 (ppm)
12. NO (cold) read/3% 02 (ppm)
13. Carbon Dioxide (%)
14. Carbon Monoxide (ppm) uncor/cor
15. Hydrocarbon (ppm) uncor/cor
16. Sulfur Dioxide (ppm) uncor/cor
17. Smoke Spot (Bacharach)
18 Atmoo Temp »C)««r gvtff
19. Dew Point Temp. ("F/eC)
20. Atmos. Pressure (in. Hg)
21. Relative Humidity (%)
22.
23.
24.
25.
26.
27.
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1 V
625
-------
MOBILE LABORATORY DATA
Test No. 12/1- 2- Date tff/fZ/7f Location £2
Unit No. /
Test No.
Fuel*/* 6A& Capacity 67
Unit Type VfAT/fAt f*ef/*t
Burner Type Ceffi) P/IZ-* 'f
1. Test Mo.
2. Date
3. Tine
4. Load
5. Process Rate
6. Flue Diam. or Size, ft
7. Probe Position
6. Oxygen (%)
9. NOx (hot) read/3% 0? (ppm)
10. NO (hot) read/3% 02 (ppm)
11. NO? (hot) read/3% Oj (ppm)
12. NO (cold) .read/3% 02 (ppm)
13. Carbon Dioxide (%)
14. Carbon Monoxide (ppm) uncor/cor
15. Hydrocarbon (ppm) uncor/cor
16. Sulfur Dioxide (ppm) uncor/cor
17. Smoke Spot (Bacharach)
pxr fviff
L8 Xt^Ba. iTteBiD f0F/°O
19. Dew Point Temp. (eF/°C)
20. Atmos. Pressure (in. Bg)
21. Relative Humidity (%)
22.
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25.
26.
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Data Sheet 6002-2
626
-------
Test No
Unit No.
MOBILE LABORATORY DATA
.. A2//-1 pate IO/l*/7( location A2_
Test No.
Engr.
\
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Unit Type_
Burner Type
1. Test No.
2. Date
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6. Flue Diam. or Size, ft
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8. Oxygen' (%)
9. NOx (hot) read/3% 0? (ppm)
10. NO (hot) read/3% 02 (ppm)
11. NO? (hot) read/3% 02 (ppm)
12. NO (cold) read/3% 02 (PPm)
13. Carbon Dioxide (%)
14. Carbon Monoxide (ppm) uncor/cor
15. Hydrocarbon (ppm) uncor/cor
16. Sulfur Dioxide (ppm) uncor/cor
17. Smoke Spot (Bacharach)
PA y $al C
18. Mmae, Tamp, (°F/°C)
19. Dew Point Temp. (eF/°C)
20. Atmos. Pressure (in. Hg)
21. Relative Humidity (%)
22.
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24.
25.
26.
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MOBILE LABORATORY DATA
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10. NO (hot) read/3% 02 (ppm)
11. HCy (hot) read/3% O2 (ppm)
12. NO (cold) read/3% 02 (PPm)
13. Carbon Dioxide (%)
14. Carbon Monoxide (ppm) uncor/cor
15. Hydrocarbon (ppm) uncor/cor
16. Sulfur Dioxide (ppm) uncor/cor
17. Smoke Spot (Bacharach)
18. nttroc. Tamp, (eF/°C)
19. Dew Point Temp. (eF/°C)
20. Atmos. Pressure (in. Hg)
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Data Sheet 6002-2
628
-------
MOBILE LABORATORY DATA
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Unit No. /
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2. Date
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8. Oxygen (%)
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10. NO (hot) read/3% 02 (ppm)
11. NO? (hot) read/3% 02 (ppm)
12. NO (cold) read/3% 02 (ppm)
13. Carbon Dioxide (%)
14. Carbon Monoxide (ppm) uncor/cor
15. Hydrocarbon (ppm) uncor/cor
16. Sulfur Dioxide (ppm) uncor/cor
17. Smoke Spot (Bacharach)
18. ft tea B. Btei&i (°F/°C)
19. Dew Point Temp. (eF/°C)
20. Atmos. Pressure (in. Hg)
21. Relative Humidity (%)
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26.
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Data Sheet 6002-2
629
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Test No. J2L/h_£__ Date
Onit No.
MOBILE LABORATORY DATA
Location 12-
Test No.
/
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Unit Type
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2. bate
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10. NO (hot) read/3% 02 (ppm)
11. NO? (hot) read/3% 02 (ppm)
12. NO (cold) read/3% 02 (ppm)
13. Carbon Dioxide (%)
14. Carbon Monoxide (ppm) uncor/cor
15. Hydrocarbon (ppm) uncor/cor
16. Sulfur Dioxide (ppm) uncor/cor
17. Smoke Spot (Bacharach)
18. Atmos. Temp. (°P/°C)
19. Dew Point Temp. (°F/eC)
20. Atmos. Pressure (in. Hg)
21. Relative Humidity (%)
22.
23.
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Data Sheet 6002-2
630
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9. MOx (tot) r*ad/3% Oa fppa)
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11, HO? (tot) mad/3* 02 (PCM)
12. W> (cold) r*ad/3% O2 (PMI)
13. Carbon Dioxida (•)
14. Carbon Monoxida (PPB) oncor/oor
5. Hydrocarbon (PPB) moor/cox
16. Bolter Dioxida (pea) tncor/cox
17. Bxoka Spot (Bacharach)
18. Ataoa. Vnp. <«r/»C)
19. Dav Point «av. (•ff/*C)
20. At*M. Peaaant* (in. Ha)
21, Malatiw BuBiditr (%)
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6002-2
631
-------
I
MOBILE LABORATORY DATA
Test VQ._'2//-f Date >f'IJ-7f—Location
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Test No.
Engr. W C,
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10. NO (hot) read/3% 02 (ppm)
11. NO? (hot) read/3% 02 (ppm)
12. NO (cold) read/3% 02 (ppm)
13. Carbon Dioxide (%)
14. Carbon Monoxide (ppm) uncor/cor
15. Hydrocarbon (ppo) uncor/cor
16. Sulfur Dioxide (ppm) uncor/cor
17. Smoke Spot (Bacharach)
18. Atmos. Temp. (0F/°C)
19. Dew Point Temp. (eF/eC)
20. Atmos. Pressure (in. Hg)
21. Relative Humidity (%)
22.
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26.
27.
28.
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Data Sheet 6002-2
632
-------
Test Ho._
unit NO.
MOBILE LABORATORY DATA
Date /0//Y/7S location 12.
Test Mo.
Capacity^
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1. Test No.
2. Date
3. Time
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16 *.tS»o *Tcmp (°P/°C)
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633
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634
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HOBII£ LABORATORY DATA
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Data Sheet 6002-2
635
-------
CONTROL ROOM DATA
Location 12
Unit 1
FCC CHARGE HYDROTREATER
Data Taken By lv/9 C
Test No.
Date
Time
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Pass 1
Pass 2
Pass 3
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Temperatures (°F)
Charge Temperature
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ID Fan Outlet
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CONTROL ROOM DATA
Location 12
Unit 1
FCC CHARGE HYDROTREATER
Data T»ken By
Test No.
Date
Time
Charge Oil Flow x 700 B/D
Pass 1
Pass 2
Pass 3
Pass 4
Hydrogen Flow to Heater
X 2.500,000 SCFD
Pass 5
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Temperatures (*F)
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CONTROL ROOM DATA
Location 12
Unit 1
FCC CHARGE HYDROTREATER
Sata Taken By W' C-
Test No.
Date
Time
Charge Oil Flow x 700 B/D
Pass 1
Pass 2
Pass 3
Pass 4
Hydrogen Flow to Heater
x 2,500,000 SCFD
Pass 5
Pass 6
Pass 7
Pass 8
Fuel Flow to Heater
x 3 MM SCFD
Fuel Oil Flow to
Heater x 80 B/D
Oxygen Analyzer (% OO
Temperatures (°F)
Charge Temperature
Heater Radiant Section
Flue Gas Duct to Air Heater
ID Fan Outlet
Convection Section
Arch Section
Combustion Air Inlet
Draft Gauges
Hindbdx Pressure, in. H?0
Stack .
Convection Top
Convection Bottom
XD Fan Outlet
Firebox Vacuum, in. ' HnO
Preheater Inlet, in. H.O
Fuel Gas Inlet, psig
Fuel Oil Inlet, psig
/*//- *
lo-/f-7S
e>if$-
7.1
7,1
7-1
7,1
6,$
f>1
£S
Mf
25~7
l?3f
lift
67f
3.1
S~l
V2-
u/l-te
te-tf-7t
H03
7-f
7.1
7.1
?.y
t.tf-
7.0
f,1
£.?
<.l
*,e
i.r
' W
1117
/070
zte
in*
n fi
676
3,0
y?
*3
/*//-//
t*'Hf~7f
I/If
7.-/1-7£
W
7.1
7.1
7.1
7.1
f.g
*,*?
f.1
7*0
./
S.r
2.3-
100
Hit
W7
2SI
1130
Htl
ffo
3.1
rr
2*
638
-------
LOCATION 12
UNIT 1
FUEL OIL ANALYSIS
Test 12/1-8 November 14, 1976
Carbon, % 87.37
Hydrogen, % 10.30
Nitrogen, % 0.27
Sulfur, % i.ie
Aah, % 0.044
Oxygen, I
(by difference) 0.86
API Gravity at 60»P 12.7
Heat of Coobuition:
Gross BTU/lb. 18,450
Net BTU/lb. 17,510
639
-------
GASEOUS FUEL ANALYSIS
Mo tZ/f-lrej Date H> -/J-74 Location >2-
Unit Mo. /
Fuel /Iff, GAS _ Fuel Sample No_
Fuel Sample toint.fi/fi.
Fuel Analysis by_
Test Mo
Engr
Gas
% CF air Btu(HHV) CF COa CF H^O CF Prod Ib Prod
Volume Cf fuei CF fuel CF fuel CF fuel CF fuel CF fuel
CH4
C3H8
c?H?n
c4°
&
r
CO
H2
Methane
Ethane
Propane
Butane
Pentane
Ethylene
Propylene
Butylene
Pentylene
Acetylene
Benzene '
Oxygen
Nitrogen
Carb. Diox
Carb. Monox
Hydrogen
x 0.0955
~x 0.1671
~x 0.2387
"x 0.3103
~x 0.3819
~x 0.1432
~x 0.2148
~x 0.2869
~x 0.3580
~x 0.1193
~x 0.3580
~x -0.0477
x 0.0239
W.f x 0.0239
9.94
17.51
25.19
33.21
41.11
15.80
23.33
31.23
39.16
14.57
38.48
3.15
3.18
0.01
0.02
0.03
0.04
0.05
0.02
0.03
0.04
0.05
0.02
0.06
0.01
0.01
0.02
0.03
0.04
0.05
0.06
0.02
0.03
0.04
0.05
0.01
0.03
0.01
0.1055
0.1821
0.2587
0.3353
0.4119
0.1532
0.2298
0.3068
0.3830
0.1343
0.3730
0.0377
0.01
0.01
0.0289
0.0289
0.000416
0.000786
0.001171
0.001548
0.001864
0.000726
0.001087
0.001449
0.001813
0.000682
0.002017
0.000828
0.000728
0.001145
0.000724
0.0000522
Total
Iff 0.00 l/.fffi
Theoretical Air:
SCF air _ CF air ,,,6 / Btu(HHV)
10° Btu " CF fuel *
CF fuel
/
/
a
1.337 2.3IZ If.efo o.oftl
SCF air/10 Btu 6 70°F,
29.92 in. Bg.
HSCF Prod
CF Prod
106 Btu CF fuel
% Moisture •
' Btu(HHV)
CF fuel
CF fuel
17.7
DSCF Prod
106 Btu
10°Btu
CF COa
(100 - % Moisture)
100
//CF Prod CF H?0 \
1 / ^CF fuel " CF fuel/
K -
331.5x10
Net SCF Prod/10 Btu
\ HO
Dty SCP/10
% oo . dry
2' ary
MH x (DSCF/106 Btu)
K* -X/430
lb/106 Btu - (ppm e 3» 02)/K
- (ppm 0 3% 02)/K'
K for
lb/106 Btu
/!££_
Data Sheet 6002-6 (Rev. 1)
640
-------
GASEOUS FUEL ANALYSIS
Test
Unit
Fuel
Gas
CH4
C2H6
C3H8
C H
C5H12
24
C3H6
C H
CgH?D
CjHT
C-H?
°2
N
Co,
CO
H2
no/2//-/ rot
No. /
Test Mo
' Date 10 -/2- 7f Location 13-
Fuel/f^/f G4l
' Fuel Sample
No
Engr
w. cure*
Sample Point/"C^V tf/fj ^(///Fuel Analysis by
Methane
Ethane
Propane
Butane
Pentane
Ethylene
Prbpylene
Butylene
( Fentylene
Acetylene
Benzene
Oxygen
Nitrogen
Carb. Diox
Carb. Monox
Hydrogen
%
Volume
(1.3 x
ftf>
l.y x
. x
X
1,3 x
/./" x
X
X
X
X
X
X
CF air
CF fuel
0.0955
0.1671
0.2387
0.3103
0.3819
0.1432
0.2148
0.2869
0.3580
0.1193
0.3580
-0.0477
0.0239
0.0239
Btu(HHV)
CF fuel
9.94
17.51
25.19
33.21
41.11
15.80
23.33
31.23
39.16
14.57
38.48
3.15
3.18
CF
CF
0.
0.
0.
0.
0.
0.
0.
0.
0.
0.
0.
0.
0.
C02
fuel
01
02
03
04
05
02
03
04
05
02
06
01
01
CF
CF
0.
0.
0.
0.
0.
0.
0.
0.
0.
0.
0.
0.
H20
fuel
02
03
04
05
06
02
03
04
05
01
03
01
CF
CF
0
0
0
0
0
0
0
0
0
0
0
-0
0
0
0
0
Prod
fuel
.1055
.1821
.2587
.3353
.4119
.1532
.2298
.3068
.3830
.1343
.3730
.0377
.01
.01
.0289
.0289
lb Prod
CF fuel
0.000416
0.000786
0.001171
0.001548
0.001864
0.000726
0.001087
0.001449
0.001813
0.000682
0.002017
0.000828
0.000728
0.001145
0.000724
0.0000522
Total
Theoretical Air:
SCF air CF a
O.0603.
CF fuel
106/BtUJHHV? ,
CF fuel
air/10 Btu 9 70°F,
92 in Hg>
WSCF Prod
106 Btu
K -
MM x (DSCF/106 Btu)
K* -K/430
6
lb/10 Btu - (ppm
ng/J • (ppm e 3% 02>/K'
3« 02)/K
Data Sheet 6002-6 (Rev. 1)
64 1
-------
Pate
oe.T *76>
K V B. INC.
SOx DATA SHEET
Test No. /g//~/Jt
TEST NO.
UNIT NO.
FUEL
LOAD
b/hr location
Box NO.
Tine
Temp, in Gas Meter
Press, in Gas Meter
Meter Reading
Barom. Press.
Percent Oxygen
N£ Purge Tine
/
/J/.4-
/*o
0
0
*9.y
a. 3
f3¥/
/
t*3x
L/2/75
642
-------
Date
oe.r '?(>
K V B. INC.
Test No.
TEST NO.
UNIT NO.
SOX DATA SHEET
FUEL */«'** LOAD
Jclb/hr
Location
Box No.
Time
Temp, in Gas Meter
Press, in Gas Meter
Meter Reading
Barom. Press.
Percent Oxygen
N2 Purge Time
2
/3s-y
/AO
0
0
a9.f
'•9
JVJ*
a, •
/V06.
//f
o
J.OOO
*?.• T) x 24
V (P + p)
A » Ml of lead perchlorate used for sample •>
B = Ml of lead perchlorate used for bland =
M - Normality of lead perchlorate titrant •*
F • Dilution factor •>
T » Average temp, in gas meter =
V '• Volume of gas sample f t3 •>
P » Barometric pressure m
p • Pressure in gas meter »
ConcentrationfCi ppm "
- Ctf 2090 |
bo.9-XO, I
Mtra 1> "
E
where
Emission-,E, g/Mcal "
Ib/MBtu •
ng/J -
C • pollutant concentration, . g/dscn .
P, volume factor - _ dscVIO cal
from P«d. Reg. 9/11/74 p 32856
Btu
so2
/V,9
s-,o
. 017*
/O
s-eo
S.ooo
Jtt.V
O
&*£
so3
—
sox
-
60-14
rev. 1/2/75
643
-------
Date
K V B. INC.
Test No.
SOx DATA SHEET
TEST NO.
UNIT NO.
FUEL
LOAD
Jclb/hr
Location
Box Ho.
Time
Temp, in Gas Meter
Press, in Gas Meter
Meter Reading
Barom. Press .
Percent Oxygen
K2 Purge' Time
/
/if so
//*
o
o
*9>Y
*¥
/?*•*-
/
/**/
//*
o
/,e>oQ
*9.tf
*>V
ts-/o
Calculation: SO. or SO-, ppm
Excess 02 >?-y %
(A - B) x K x F x (460 ^, T) x 24
V (P + p)
A » Ml of lead perchlorate used for sample «
B - Ml of lead perchlorate used for bland «
N - Normality of lead perchlorate titrant =
P «• Dilution factor »
T - Average temp, in gas meter «=
V » Volume of gas sample ft3 •
P * Barometric pressure »
p - Pressure in gas meter «
Concentration,C, ppm •=
E - oT 2090 1
bo.S-xOjl
where L J
Emission-,E, g/Mcal •
Ib/HBtu *
ng/J -
C - pollutant concentration, g/dscm
P, volume factor - _dsem/10 eal
«*cina*
from Fed. tog. 9/11/74 p 32856
so2
sy.sr
jr.o
.owl
/o
-S-72
/xftdO
29.
16/
SO3
•
•
sox
60-14
rev. 1/2/75
644
-------
PETROLEUM PROCESS HEATER
Location No. | ^_ _ Unit No.
Unit Description ~Pe.TeoL.eOhl "PeoC£€>S UEACTS.R.
VERTICAL, Foece^T^e^FT De UexAMi
Installation Date 19 (o
Heater Rating IO J
Burner Description
CO £-V^ "^)Ofc^ Eg> T)A.Z
Test Fuel Combinations rC.
Fuel Temp, at Burner (°F) . KJ.CpQlU 5C>1 VC C2OO
Primary Air Temp. (°F)
Comments:
645
-------
MOBILE LABORATORY DATA
Test No. /2/2-/ Date 10 //?/?£ Location
Test No.
Unit No.
Fuel
Capacity_
Unit Type
Burner Type
1. Test No.
2. Date
3. Time
4. Load
5. Process Rate
7. Probe Position
8. Oxygen (%)
9. NOx (hot) read/ 3% 03 (ppm)
10. NO (hot) read/3% 02 (ppm)
11. NO? (hot) re ad/ 3% 02 (ppm)
12. NO (cold) read/3% 02 (ppm)
13. Carbon Dioxide (%)
14. Carbon Monoxide (ppm) uncor/cor
15. Hydrocarbon (ppm) uncor/cor
16. Sulfur Dioxide (ppm) uncor/cor
17. Smoke Spot (Bacharach)
18. Atmos. Temp. (6F}0C)
19. Dew Point Temp. <^F)°C)
20. Atmos. Pressure (in. Hg)
21. Relative Humidity (%)
22.
23.
24.
25.
26.
27.
28.
29.
30.
'2/2 -/
K>//f/7t
/ :0rrn
Rer. GAS
STACK
<•!.
*5~0
WO
20
/f1
7,
0
qo
3
1(2.
Ho
3-2-
/£Z
2-
0
77
V7
V/
21-3*1
6&
12/2-2
W//?/76
3'** M
#£ OIL
ZTJCK
H.3
123
120
3
I55~
//-
20
2-ZO
>3?
)2<\
i
1(7
?
22
302
\
'
I
<
•
•.
646
Data Sheet 6002-2
-------
MOBILE LABORATORY DATA
Test No. & /2 -3 Date K>//t/76 Location / -2-
Test No.
Engr
unit NO.
FuelJt£F,J$A$_ Capacity_
Unit Type
Burner Type
1. Test No.
2. Date
3. Time
4. Load
5. Process Rate
6. Flue Diam. or Size, ft
7. Probe Position
8. Oxygen (%)
9. NOx (hot) read/3% 02 (ppm)
10. NO (hot) read/3% 02 (ppm)
11. NO? (hot) read/3% 02 (ppm)
12. NO (cold) read/3% 02 (ppm)
13. Carbon Dioxide (%)
14. Carbon Monoxide (ppm) uncor/cor
15. Hydrocarbon (ppm) uncor/cor
16. Sulfur Dioxide (ppm) uncor/cor
17. Smoke Spot (Bacharach)
JPK f a *r ff fff f*^\.
19, Dew Point Temp. (S/'C)
20. Atmos. Pressure (in. Hg)
21. Relative Humidity (%)
22,
23.
24.
25.
26.
27.
28.
29.
30.
a/2-3
19 //?/?£
tfiivAtf
fr/f-cx
y.
—
fg
•—. .
—
t*.
2V
to
0
._
72^
— .
—
£
2?
VZ.
12/2. -3
>*//f/?S
7//3V/7
smx
3,7
&
h/J
£?
#3
$,
/i
to
£2.
f£
o
16
q
/?
62.
?f
32-
2*1,71
£S~
-^ SA $S
)Z/2-3
>0//f/7£
it'lofrt
*nc/<
?,
S6
t?
/
1*
1-
>t
7*
q
/f
/^
/
?r
f
/f
?*/
;2-/2 - 3
>Q//f/7S
2'io Pn
*r*c/<
v.
So
Sc>M7£
}'.5~0
*T y.4^ JLS
^ /Xv"*-*x
3.S
te £3
fo {$
0 O
78 %2
*f.3-
f *
2^ 2j
^f. (#
647
Data Sheet 6002-2
-------
MOBILE LABORATORY DATA
Test No. 12/2 "3 Date I0//2/7S Location )
Test No.
Engr.
Unit No.
Capacity_
Unit Type
Burner Type
1. Test No.
2. Date
3 . Time
4. Load
5. Process Rate
6. Flue Diam. or Size, ft
7. Probe Position
8. Oxygen (%)
9. NOx (hot) read/3% ©2 (ppm)
10. NO (hot) read/3% 02 (ppm)
11. NO? (hot) read/3% 02 (ppm)
12. NO (cold) read/3% 02 (ppm)
13. Carbon Dioxide (%)
14. Carbon Monoxide (ppm) uncor/cor
15. Hydrocarbon (ppm) uncor/cor
16. Sulfur Dioxide (ppm) uncor/cor
17. Smoke Spot (Bacharach)
P/?f 0010 s-^
IB Al^nwn -iJtemci. ff'F/TM
19. Dew Point Temp. d^°C)
20. Atmos. Pressure (in. Hg)
21. Relative Humidity (%)
22.
23.
24.
25.
26.
27.
28.
29.
30.
&/Z-3
IO//3/76
5-:y0sn
mcK
3.7
5~t
rf
FZ
ft
G
?$
f
^
y^
i<>
3?
21.£f
X3
•
r
648
Data Sheet 6002-2
-------
Test No . 12- /2 ~
Unit No.
MOBILE LABORATORY DATA
H>//4/76 Location _ X.2
Test No.
Engr .
Fuel/?/Of
acity
Unit Type
Burner Type
-/^'7^
If 100'
4? y A f** ^
^ / ff Q-. A^
5,
107
£t 4f
7
130
f.
V?
—
foo
£>
in
1/0
#
f *[ Q
£1
*ff*~
•
tt3
f
^2-
f£>
z^ri
^F *
& D
\
_
Data Sheet 6002-2
I
-------
MOBILE LABORATORY DATA
Test No. I2-/3- ~~ g Date /0-2O-76 Location 12-
Unit No. Fuel R£f, £4$ Capacity
Test No.
Engr.
Unit Type
Burne r Type
1. Test No.
2. Date
3. Time
4. Load
5. Process Rate
6. Flue Diam. or Size, ft
7. Probe Position
8. Oxygen (%)
9. NOx (hot) read/3% 0^ (ppm)
10. NO (hot) read/3% 02 (ppm)
11. NO? (hot) read/3% 02 (ppm)
12. NO (cold) read/3% 02 (ppm)
13. Carbon Dioxide (%)
14. Carbon Monoxide (ppm) uncor/cor
15. Hydrocarbon (ppm) uncor/cor
16. Sulfur Dioxide (ppm) uncor/cor
17. Smoke Spot (Bacharach)
18. Atmos. Temp. (°%}°C)
19. Dew Point Temp. (*F}°C)
20. Atmos. Pressure (in. Hg)
21. Relative Humidity (%)
22.
23,
24.
25.
26.
27.
28.
29.
30.
&/Z-6
10 -J0 -76
t/'V?
61" IP
irAc#
?,.
H3
/C3
/&
/If
/0
#
—
70
3
//?
I**
fO
13-7
,3
0
—
71
it *?
£V M
zi' -if
72
&fc~f
IP -20'?*
/f;00
6v" 'ID
*rAc/<
3.
103
/03
0
12*
?•-
^
—
io
—
?
f0S
/o%
&
I??
r
^
—
12-
y?
y^
21-i6
ft
12/2-6
10-20-76
ft'-**
6l"lt>
srAtfti
t'
//£>
/£>$
2.
l?0
1'
f
—
6
-------
MOBILE LABORATORY DATA
Test No. !2/2-~7 Date IO-26-7J Location V.2-
Test No.
Unit No.
Fuel
S
Capacity
Unit Type
Burner Type
1.' Test No.
2. Date
3. Time
4. Load
5. Process Rate
6. Flue Diam. or Size, ft
7. Probe Position
8. Oxygen (%)
9. NOx (hot) read/ 3% O^ (ppm)
10. NO (hot) read/3% 02 (ppm)
11. NOp (hot) read/3% 02 (ppm)
12. NO (cold) read/3% 02 (ppm)
13. Carbon Dioxide (%)
14. Carbon Monoxide (ppm) uncor/cor
15. Jiydrocarbon (ppm) uncor/cor
16. Sulfur Dioxide (ppm) uncor/cor
17. Smoke Spot (Bacharach)
18. Atmos. Temp. (°F/°C)
19. Dew Point Temp. (°F/°C)
20. Atmos. Pressure (in. Hg)
21. Relative Humidity (%)
22.
23.
24.
25.
26.
27.
28.'
29.
eo.
I2-/2- 7
10 -2(, '-7*
<23
f*
/2-A-7
lo-2
l'7<
/0:
-------
Test No. I2-/2 %
Unit No.
MOBILE LABORATORY DATA
Location
Test No.
Engr.
Fuel_fV_£/£_ Capacity
Unit Type
Burner Type
1. Test No.
2. Date
3. Time
4. Load
5.' Process Rate
6. Flue Diam. or Size, ft
7. Probe Position
8. Oxygen (%)
9. NOx (hot) read/3% 03 (ppm)
10. NO (hot) read/3% 02 (ppm)
11. NOj (hot) read/3% 02 (ppm)
12. NO (cold) read/3% 02 (ppm)
13. Carbon Dioxide (%)
14. Carbon Monoxide (ppm) uncor/cor
15. Hydrocarbon (ppm) uncor/cor
16. Sulfur Dioxide (ppm) uncor/cor
17. Smoke Spot (Bacharach)
18. Atmos. Temp. (°F/°C)
19. Dew Point Temp. (°F/°C)
20. Atmos. Pressure (in. Hg)
21. Relative Humidity (%)
22.
23.
24.
25.
26.
27.
28.
29.
30.
i x» j*y ^ fy
/, ^£ f ^^ o
/> 'Jt'76
12 '-2-0
—
—
$r*c*
$-,
125
///
7
151
7.
20
/£>
it
7
ITS
?
23
//
&t
13
ye
3s, 3
'71
ti/2-?
W-~J('7f
l2-'/£>
—
—
STACK
^
&1
120
• —
- —
?r+cKi
3.f~
12 f
)23
/
///
//
3"
0
V7*
•f.0
130
&
-------
CONTROL ROOM DATA
Location 12
Unit 2
DEHEXANIZER
Data Taken By
Test No.
Date
Time
Reboiler Feed Rate x 1700 B/D
Pass A
Pass B
Pass C
Pass D
Fuel Gas to Reboiler x 108 MSCFD
Oxygen Analyzer (% 0,)
Temperatures (°F)
Combined Outlet
Ho. 1 Outlet
No. 2 Outlet
No. 3 Outlet
No. 4 Outlet
Stack
Convection Section (top)
Convection Section (bottom)
Radiant Section
Fuel Oil (gauge)
Pressure Gauges
Windbox Pressure, in. H,0
Steam/Fuel Oil Differential
Pressure, psig • • '
Fuel Gas Supply, psig
Fuel Gas Inlet, psig
Fuel Oil Pressure, psig
Fuel Oil to Burner, psig
U/2-/
t0-lf-%
iis-s~
5"
r
r
r
.7*
r.3.
317
?1I
391
H?
Ill
m
57*
I3.5~l
goo
—
,re>
3f
31
o
—
I2-/2.-2-
(0-15-7*
/iff
r
5-
5-
S"
.30
r.7
3S7
3?1
}*?
313
311
FHI
r/3
/*t1
fS-7
2/2
,3g
20
?£
5*
5-o
•il
V
653
-------
CONTROL ROOM DATA
Location 12
Unit 2
DEHEXANIZER
Data Taken By
Test NO.
Date
Tine
Reboiler Feed Rate x 1700 B/D
Pass A >
Pass B
Pass C
Pass D
Fuel Gas to Reboiler x 108 MSCFD
Oxygen Analyzer (% O,)
Temperatures (°F)
Combined Outlet
No. 1 Outlet
No. 2 Outlet
No. 3 Outlet
No. 4 Outlet
Stack
Convection Section (top)
Convection Section (bottom)
Radiant Section
Fuel Oil (gauge)
Pressure Gauges
Windbox Pressure, in. H^O
Steam/Fuel Oil Differential
Pressure, psig
Fuel Gas Supply, psig
Fuel Gas Inlet, psig
Fuel Oil Pressure, psig
Fuel Oil to Burner, psig
12/2- 3
ie//t/7f
/0:aS~
5~
S
5
f
f.2.
5~.o
??£
3tt
3*7
31Z
It*}
s'if
f/1
12 Y5~
*I3
2io-ffff
a/?
22. S-
rt
ry
—
—
12 /Z- 3
IP//Z/7*
I2H1
r
5"
5-
r
f.3
i.1
?*7
Jfl
1ft
?13
310
ryf
f/3
1237
ZI2
—
0,07
22.?
$**
Tf
a/2 -J
t*//t/7t
3'-ff
r
F
F
r
f.3
f.o
3Zf
3*1
3tf
I'M
31?
fi7
ft
123 ?
ZI1
_
0.3S"
23-0
£0
5-f
•
12/2'J
10/18/76
fiOO
f
f
r
r
S.3
i.i
w
381
3*8
313
310
FK
f/3
HW
1IX
—
0.3$-
zz..?
ff.ff
fl
•
•
654
-------
CONTROL BOOM DM*
Location 12
Unit 2
DEHEXMIXZER
Data Taken By
Test No. .
Date
Time
Reboiler Feed Rate x 1700 B/D
Pass A
Pass B
Pass C
PaSB D
Fuel Gas to Reboiler x 108 MSCFD
Oxygen Analyser (% 0«)
Temperatures (CF)
Combined Outlet
Ho. 1 Outlet
No. 2 Outlet
No. 3 Outlet
No. 4 Outlet
Stack
Convection Section (top)
Convection Section (bottom)
Radiant Section
Fuel Oil (gauge)
Pressure Gauges
Windbox Pressure, .in. HjO
Steam/Fuel Oil Differential
Pressure, psig
Fuel Gas Supply, psig
Fu-al CE.C Inlet, psig
' Fuel Oil Pressure, psig
Fuel Oil to Burner, psig
U/-2-V
IO//1/7*
0111
r
f
r
y
f.i
•t.z
3tg
31o
391
31i
. 310
5-1J.
W
I2S£
f/i
—
0,2 f
22.. 5"
&.*
5*1.0
«/*-?
lo/H/7f
lotf
/-
f
r
r
*.l
1.3
3g7
31*
Wt
31V
311
Flff
F07
IZfo
9/0
—
— -
2.3..F
F7.5
5-1,0
—
—
A2/2-5*
i*//i/r*
I60t>
r
r
$
r
3.Z
f.3
3fg
?31
3S1
3W
31/
ttz
&1
1/7*
131
t?7 -
1.*?
23.0
r*.?
S"2..0
10
ft
'j.
"
655
-------
CONTROL ROOM DATA
Location 12
Unit 2
DEHEXANIZER
Data .Taken By
Test No. .
Date
Time
Reboiler Feed Rate x 1700 B/D
Pass A
Pass S
Pass C
Pass D
Fuel Gas to Reboiler x 108 MSCFD
Oxygen Analyzer (% 0,)
Temperatures (°F)
Combined Outlet
No. 1 Outlet
No. 2 Outlet
No. 3 Outlet
No. 4 Outlet
. Stack
Convection Section (top)
Convection Section (bottom)
Radiant Section
Fuel Oil (gauge)
Pressure Gauges
Windbox Pressure, in. HnO
Steam/Fuel Oil Differential
Pressure, psig
Fuel Gas Supply, psig
Fuel Gas Inlet, psig
Fuel Oil Pressure, psig
Fuel Oil to Burner, psig
12/2-t
lefee/rt
113^*1
r
r
r
y
6J^
H.i
3*1
110
3*1
W
311
nz
$~0S
IZ£1
til
— -•
0.3*
Zf.o
£0,0
&.0
•
/*/2-/
/e/2e/7S
lit? PM
5-
f
r
5"
«-5-
V-3
3f7
3?1
3ff
313
3 SI
r*7
r*i
IZt7
t»i
—
0.j./7S
Iff?
f
5~
r
r
*2~f
i.i
•
3tt
3tt
397
311
3*1
?32
F0/
/at
10*
—
e.*i
28, e>
FT,*
fl.0
.
—
656
-------
CONTROL 'ROOM DATA
location 12
Unit 2
DEHEXANIZER
Data Taken By
Test No.
Date
Tine
Reboiler Feed Rate x 1700 B/D
Pass A
Pass B
Pass C
. Pass D
Fuel Gas to Reboiler x 108 MSCFD
Oxygen Analyzer (% 0,)
Temperatures (°F)
Combined Outlet
No. 1 Outlet
No. 2 Outlet
No. 3 Outlet
No. 4 Outlet
Stack
Convection Section (top)
Convection Section (bottom)
Radiant Section
Fuel Oil (gauge)
Pressure Gauges
Windbox Pressure, in. H..O
Steam/Fuel Oil .Differential
Pressure, psig
Fuel Gas Supply, psig
Fuel Gas Inlet, psig
Fuel Oil Pressure, psig
Fuel Oil to Burner, psig
A2/2-7
ie>/*
f3fO
—
— -~
H/2.-7
/0/2(/7f
0137
r
—
—
«/i-7
l'fa/7{
/0/e>
f
f
f
f
7S.0
1.0
3*7
310
381
311
311
K2-
5~J-1
IJ-13 •
732
*.I1
. . —
5~£.0
f^.e>
— .
, —
X2/2-7
/»/2f/r(
lloo
r
f
^
5-
7^0
5:8
310
31/
319
3?f
312
?2<
•f11
I26f
932.
• —
0.1 0.
- —
F7.0
$-3.0
• —
657
-------
CONTROL ROOM DMA
Location 12
Unit 2
DEHEXANIZER
Data Taken By
Test No.
Date
Tine
Reboiler Feed Rate x 1700 B/D
Pass A
Pass B
Pass C
Pass D
Fuel Gas to Reboiler x 108 MSCFD
Oxygen Analyzer (% 0*)
Temperatures (°F) .
Combined Outlet
No. 1 Outlet
No. 2 Outlet
No. 3 Outlet
No. 4 Outlet
Stack
Convection Section (top)
Convection Section (bottom)
Radiant Section
Fuel Oil (gauge)
Pressure Gauges
\
Windbox Pressure, in. H*O
Steam/Fuel Oil Differential
Pressure, psig
Fuel Gas Supply, psig
Fuel Gas Inlet, psig
Fuel Oil Pressure, psig
Fuel Oil to Burner, psig
H/2-3
lt>/*f/7S
A2/Y
r
5-
5"
y
3-1
?,<
3rv
?ei
W
311
311
?(7
tto
ni7
Iff
*//
0<10
30,0
5-8.5*
r?,o
zr.s*
20,0
H/2-3
lefef/H
ta.fi
f
T
?
r-
• 3,0
f'2.
3*1
311
3M
3H
311
£7f
&S
it ft
1(S
101
ff.ff-
30,0
&.?
rs,*
*£•,$-
10. 0
&/*-?
te/2£/7f
&23
s-
r
r
5"
2.0
t.£
3gf
3*1
381
311
311
m
rst
1112.
17*
3>0g
0,17
90,0
tt.f
rr.s-
zr.s*
20,0
ate-?
t0/a.g/rt
I3f0
r
5"
f
5*
1.0
i.t
j*t
3tt
3Z1
3?J
27/
ttJ
r>?
tin
170
2*08
0,1?
3*,0
f7.f
/r,r
^/rr
3.0,0
658
-------
Test 12/2-2
LOCATION 12
UNIT 2
NO. 6 FUEL OIL ANALYSIS
November 15, 197(
Carbon, %
Hydrogen, %
Nitrogen, Z
Sulfur, t
Ash. X
Oxygen, %
(by difference)
API Gravity at 60*F
Beat of Combustion:
Groat BTU/lb.
Net BTU/lb.
87.22
10.33
0.27
1.14
0.035
1.00
12.6
18,380
17,440
659
-------
LOCATION 12
UNIT 2
FUEL GAS CHROMATOGRAPHIC ANALYSES
The six samples of gas were marked as follows:
1.
2.
3.
4.
5.
6.
Test
Test
Test
Test
Test
Test
12/2-4,
12/2-3,
12/2-3,
12/2-1,
12/2-6,
12/2-6a.
1115
1630
1300
1300
1400
1400
hrs.
hrs.
hrs.
hrs.
hrs.
hrs.
10-19-76
10-18-76
10-18-76
10-15-76
10-20-76
10-20-76
Samples #5 and #6 had the sane identification, so an "A" was added to the
last sample number. It arrived with a pressure of 1 atmosphere, ao it nay have
leaked en route.
The following table summarizes the results of the gas chromatographic
analyses expressed as per cent by volume:
Oxygen
Nitrogen
Carbon Dioxide
Carbon Monoxide
Hydrogen
Methane
Ethylene
Ethane
C3 Hydrocarbons
C4 Hydrocarbons
C5 Hydrocarbons
C6 Hydrocarbons
Beating Value
(BTO dry/SCF)
0.031
2.29
0.013
0.09
54.4
19.0
5.71
9.69
6.05
2.07
0.41
0.22
0.025
0.95
0.013
< 0.04
53.3
19.9
6.12
10.3
6.39
2.23
0.48
0.28
0.034
2.40
0.013
0.04
52.9
17.8
6.30
11.0
6.61
2.16
0.46
0.24
0.023
1.00
0.013
0.07
51.2
18.5
5.21
9.87
11.4
2.11*
0.42
0.22
0.023
0.86
0.013
< 0.04
53.8
16.7
6.24
11.1
8.35
2.16
0.45
0.29
10.1
38.1
0.052
< 0.04
17.9
12.8
4.41
7.70
6.62
1.69
0.34
0.22
879
921
915
996
953
637
BOTB; The high hydrogen content required a separate gas chronatographlc analysis.
660
-------
I. f
PARTICULATE EMISSION CALCULATIONS
Test tto. >2/2-S~ Date te-/1'7f Location /2-
0/£ Sampling Train and Method
Engr.
Chit No.
Pitot Factor, Fs
Fuel
Barometric Pressure, P
\ in. Hg
Tot. Liquid Collected, V /ff5" ml Total Particulate, M /f £• ff m gm
- ^^fc^^-.^^^™.^^^™^^ B """'
Velocity Head, AP > *?.? iwg Stack Tea?). , Ts /^/^ *R Stack Area,
Sample Volume, V»__£^__ft3 Stack Press., Psg ~. 7J iwq Excess O , XO »
Orifice Press. Dif £. , H , j$ iwg Stack Gas Sp. Gravity, Gs___/L£__n.d.
Sample Time, 6/3-0 min Nozzle Dia., Dn
in. Meter Temp., T
•1. Sample Gas Volume Vm .- 0.0334 Vm(P + H/13.6)
2. Water Vapor Vw . - 0.0474 V
3. Moisture Content Bwo - Eq. 2/(Eq. 1 + Eq. 2)
SCF
4. Concentration a. C • 0.0154 Mn/Vm
•td
b. C • 2.205 x 10"6 MnAm
c. C - Eq. 4b X 16.018 x 10
•td.
3
///f
5. Abs. Stack Press. Pa - V x 13.6 + Psg
6. Stack Gas Speed Vs • 174 Fs /APTs yr^
7. Stack Gas Flow a. fisw • Eq. 6 x As x ~P. x 22_
Rate 0 70"F TS 407
b. Qsd - Eq. 7a x (1. - Eq. 3)
Ms • Eq. 7b x Eq. 4b x 60
J»2f - 2090/(20.9 - X>2%)
«. E - Eq. 4b x Fe x Eq. 9
N.D.
grains/DSCF
Ib/DSCF
grams/DSCM
in. w abs.
ft/min
WSCF/min
DSCF/min
8. Material Flow
9. X02 factor
10. Emission '
11. % Isokinetic
b. E • Eq. 4c x Fa x Eq. 9 x 1000
.14077 x T»(Vm ' + Vw ..)
z . S _2
6 x Vs x Ps x Dn
Ib/MKBtu
, ^5*5" ng/ joule
%
Fe SC Feet/104 Btu
Fm SC Meters/104 joules
Oil
92.2
0.002475
Gas
87.4
0.002346
Coal
98.2
0.002636
•Multiply Vta
by 530/T (*R) if meter not temp, compensated.
m
Data Sheet 6002-4
66 1
-------
Test No.
Unit No.
PARTICULATE EMISSION CALCULATIONS
Date /Q~ff~7f Location 12-
Fuel &£ 0fl- Sampling Train and Method
Engr.
Pitot Factor, Fs
Barometric Pressure, P
-in. Hg
Tot. Liquid Collected, V / $5~ ml Total Particulate, Mti
Velocity Head, AP_1£-£___iwg Stack Temp., Ts_/£££__°R Stack Area, As
2
Sample Volume, Vm_££_ft3 Stack Press., Psg "V ^J j^g Excess 0, XO
Orifice Press. Dif f . , H
Sample Time, 6
iwg Stack Gas Sp. Gravity, Gs /,
min Nozzle Dia., Dn X?-
n.d.
in. Meter Temp., T
•1. Sample Gas Volume Vm . . - 0.0334 Vm(P. + H/13.6)
sta bar
2. Water Vapor Vw . . - 0.0474 V,
sta Ic
3. Moisture Content Bwo • Eq. 2/(Eq. 1 -f Eq. 2)
5~f'7f $CF
_^__— ^^
SCF
,12% N.D.
4. Concentration a. C - 0.0154 Mn/Vm
std
b. C - 2.205 x lo"6 Mn/Vm
c. C - Eq. 4b x 16.018 a 10
.0J2Y2. grains/DSCF
std
3
5. Abs. Stack Press. Ps - P x 13.6 + Psg
grams/DSCM
in,, w abs.
6. Stack Gas Speed Vs • 174 Fs /APTs J^-
7. Stack Gas Flow a. Qsw • Eq. 6 x As x —— x •rr=-
Rate 8 70eF
b. Qsd • Eq. 7a x (1. - Eq. 3)
8. Material Flow
9. X02 factor
10. Emission
11. % Isokinetic
Ms - Bq. 7b x Eq. 4b x 60
K)2f - 2090/(20.9 - K>2%)
a. E » Bq. 4b x Fe x Bq. 9
b. E - Bq. 4c x Fm x Bq. 9 x 1000
14077 x T»(Vm ^ + Vw _)
I • JT
0 x Vs x Ps x Dn
WSCF/mln
DSCF/min
Ib/hr
3l.(5'5' ng/joule
Fe SC FeeVIO4 Btu
Fm SC Meters/104 joules
Oil
92.2
0.002475
Gas
87.4
0.002346
Coal .
98.2
0.002636
•Multiply Vm .. by 530/T (*R) if neter not temp, compensated.
StQ II
Data Sheet 6002-4
662
-------
PARTICUIATE EMISSION CA1CUIATIONS
Test Ho. /.Z/2-J
Unit Mo. 2-
Pitot Factor, Fs
Tot. Liquid Collec
Velocity Bead, AP
Date (6
Fuel/*.
0.93
ted- vi~
'-/r-Sf Location A*
^/f (asfS Sampling Train and Method
Barometric Pressure, P. J27- ^"7*
.2^5"? nl Total Particulate, Mft
iwg Stack Temp., Ts /^f *R Stack
Bngr.
. in. Bfl
„ a gm
•.
Area, As 22*3 /ft2
-Sample Volume, Vm V/X.^X/ft3 Stack Press., Pag -» // iwg Excess 0,, XO % ' \
Orifice Press. Diff. , B A ^ iwg Stack Gas Sp. Gravity, Gs /
n.d.
Sample Time, 6_/££__min Nozzle Dia., Dn
•1. Sample Gas Volume Vm . . • 0.0334 Vm(P.
sto bar
2. Water Vapor Vw . - 0.0474 V
3. Moisture Content Bwo - Eq. 2/(Eq. 1 + Eq. 2)
in. Meter Temp., T 5~/j
4. Concentration a. C - 0.0154 Mn/Vn
~6
std
b. C - 2.205 x 10 Mn/Vm
c. C - Eq. 4b x 16.018 » 10
'std
3
5. Aba. Stack Press. Ps " Pfcar x 13.6 + Psg
6. Stack Gas Speed Vs - 174 Fs /APIs J®- x ^—P.
7. Stack Gas Flow a. fisw » Bq. 6 x As x |3£ X'£S-
Rate « 70«F T* 407
b. Qsd " Eq. 7a x (1. - Bq. 3)
8. Material Flow Ms » Bq. 7b x Bq. 4b x 60
9. XO. factor
10. Emission
11. % Isokinetic
XOjf - 2090/C20.9 • XD2%)
a. B
-------
PARTICULATE EMISSION CALCULATIONS
Test Vo.12/2-6 v*t*/'-20-7f Location >3-
Unit No. -2-
Engr.
Pitot Factor, Fs 0.
Tot. Liquid Collected, V
Sampling Train and Method
Barometric Pressure, P
ml Total Particulate, M
_in. Hg
m gm
Velocity Head, AP ^, 03- iwg Stack Temp., Ts_/££^__°R Stack Area, As^2.2..?/ft
»
Sample Volume, Vto.3f3.0l1 ft3 Stack Press., Psg_3L^£__iwg Excess O , XO % J>
Orifice Press. Dif f . ,
Sample Time, 6 3^
*1. Sample Gas Volume
2. Water Vapor
"^, Moisture Content
4. Concentration a.
b.
c.
5. Abs. Stack Press.
6. Stack Gas Speed
7. Stack Gas Flow a.
Rate 6 70°F
b-
8. Material Flow
9. XO factor
10. Emission a.
b.
11. % Zsokinetic
H
min
- ^ ^ —
A & iwg Stack Gas Sp. Gravity, Gs / n.d.
Nozzle Dia., Dn //( in. Meter Temp., T_ $~/g °R
Vm - 0.0334 Vm(P. + H/13.6)*-^
std bar f/6
Bwo » Eq. 2/(Eq. 1 -I- Eq. 2)
C - 0.0154 Mn/Vm
eta
C - 2.205 x 10"6 Mn/Vm .
sta
C - Eq. 4b x 16.018 x 103
Ps - Pfc-r x 13.6 + Psg
Vs •
PSW
Qsd
Ms •
E "
E -
I -
• 174 Fs /APTs J^- x -ig2£
-Eq. 6xAsx|^x|2_
• Eq. 7a x (1. - Eq. 3)
« Eq. 7b x Eq. 4b x 60
E « 2090/(20.9 - X02%)
Eq. 4b x Fe x Eq. 9
Eq. 4c x Fm x Eq. 9 x 1000
14077 x Ts(Vmetd + Vwsta)
i
- $47. /f . SCF
5~f.(3 SCF
,/J^ -N.D.
grains/DSCF
Ib/DSCF
grams/DSCM
37ef,^S' in. w abs.
/7^~ ft/min
77 S2- wsCF/min
^"Y^ ^ DSCF/min
ib/hr
I.2l5~ N.D.
Ib/MMBtu
ng/ joule
/7f %
6 x Vs x Ps x Dn
Fe SC Feet/104 Btu
Fm SC Meters/104 joules
Oil
92.2
0.002475
Gas
87.4
0.002346
Coal
98.2
0. 002636
•Multiply Vm _. by 530/T ("K> if meter not temp, compensated.
Data Sheet 6002-4
664
-------
Test Bo. 12/2 ~ 5"
Box No.
Test Description pMr,c
PARTICULATE CALCULATION SHEET
Date OCT, t1K. 8L4HK.
Beaker No. 2 fO 5~ ? q
Date . .
Weighed >o/>1f7e
Tare 1 lot. Uftfi
Wt. 2 lol.lggg
3 101,1726
4 —
5 -
6 —
Avtj iei.tt?V7
Bottle No. 1*1
Impinger
Content (Water)
Rinse (ml) 65"0
Date Weighed
or 250 Bake I0'2I~7S
Final 1 toy.. 007V
Wt. 250 2 103.. 0071
3 /03-. 0030
4
5
6
Avg 10 3.. 007 g
Residue wt
Final 250-Tare .0WI
Date Weighed
or 650 Bake
Final 1
Wt. 650 2
3
4
"*S
-.6
Avg
Residue Wt
Final 650-Tare
I0/>q/7f .
too.JS_13
too. 1310
too.1387
—
—
—
100, 1J70
2
Probe
(Acetone)
If*
ip-zi-n
tea, if iff
loo. 1tl3
too.1800
loo, 7//J
.01 '23
»/lf/7f
13. 1i '03
1/.1V02-
H-1S17
—
—
• —
19,1101
3
Probe
(Water)
3. 00.
io-21-rt
m. try 3
1f. 1S~YV
If. 15 13
"
If.- If 1)
.0113.
•
,
i°/l1/7£
11, 3393
11.3333
H.iJttl
—
—
—
11. 3 3?$
**€icclone^"^
^^Rce toftejL^
3.00
it -21-7*
Tj.33.
11. 335-1
11. 33S~Y
11. 33"f g
19, 33ft
X
»/nfa
lop.1813
oo.lttl
JOO.Ifgf
—
—
—
tee.lpio
^SSC
300
IO-2I-7C
lee./ffi
teo.lggf
iee./g!7
100.1110
X
'
Filter
K/Hfa
0. 8013
0. fff/3
o, &OI3
—
—
—
. XOI3
/o-jf-r<
0.1 If 0
.13.28
.12 3 S
.12.31
JZZ£
-
Blank
No.
10
fO//1 /7f
O. VP7g
0.8071
O.3071
—
—
—
.8071
/0-2l'7t
.8083
.gogi
.30SC
,gof)
i-.oooz.
Oonanentst
Data Sheet 6002-3
665
-------
fZ.
PLANT
LOCATION
OPERATOR"
DATE iff.
RUN NO.
SAMPLE BOX NO.
nETER BOX NO. *
4ETER H ~~
5 CCMIMOUU CONSOLE RBkDXMGS
76
/3./CZ-
AMBIENT TEMPERATURE
BAROMETRIC PRESSURE ~
ASSUMED MOISTURE, % ~
HEATER BOX SETTING ~
PROBE LENGTH, IN.
NOZZLE DIAMETER, ,IN,~
PROBE HEATER SETTING*"
SCHEMATIC OF STACK CROSS SECTION
Traverse
Point
Huafcer
TOTAL
WERAGE
aeOlpl.xng
Time
fefMi*.
ClocK
r/ff£
IF31
t?5~f
ltf
tie
sure
B>'
Hg.
'3
r
Stack
Tempera-
ture
(»a)»P
<2e>
fOF
fffO
J0S-
g(1
Velocity
Head
.».»
.03
,°3
.03
.01
.01
•
Pressure
Differen-
tial Acro£
Orifice
Meter
(AH),
In. H2O
.yf
.if
.Ht
.HI
.ff
s Gas
Sample
Volume
Hfrtx *£*»*
tvn) ft3
IfVo. 3$~
irmr
iS-ff. If
irn.33~
I6oo. If
Gas S
Pemperat
>ry Gas
Inlet
(M?->
ample
ure at
Meter
Outlet
•P
60
70
72.
&r
#0
AVG.
AVG.
Sample
Box
remprta-
ture
•F
2?0
3*0
3/f
12*
3ft>
AVK
Temperature
of Gas
Leaving
Condenser on
[rftst Impinger
•F
-------
PLUME OPACITY OBSERVATION RECORD;
LOCATION NO.
OWNER
DATE
r- /t.
POINT OF EMISSION
POINT OF OBSERVATION /5~O
OBSERVER
BOILER NO.
•/FUEL
Test Run No.
CAPACITY
Xlb/hr
BURNER TYPE
TEST
No.
•
Time
ara/pm
K*0o
IS--*?
If: to
ic-ir
It- -20
K',1*
16 '30
It'.?*
K'-iO
-Type
PART 1C..
\
*
Test
Load
k«/hr
Opacity
%
10
10
Iff
1C
Iff
10 I
10
/•*
/*
WIND
Speed
inpn
5~
\
•
Direct-
SovrH
\
Sky
Cond.
awtf
\
f
Sun
Posi-
tion
—
__^.
—
—
—
—
—
—
—
Comments
•
667
-------
frarojeeti^
•Dates
Locationi_
'onits
Tests
Fuels
VELOCITY TRAVERSE
Test Descriptions
12.
Stack Cross Section
Personneli
Barometric Press, (in. 89) >
Absolute Static Press, in Stack (in. Bg)i_
Pitot Tubs Coefficients
(P.)
• 85.46 Cp
=0.7J;(
Time
•
•
Traverse Point
Port Depth
(/«.)
3
10
'1
f5~
n
61
Velocity
Bead
(in. B,0)
OP
.01 .07
.01 .07
.Of .01
.01 .10
.01 JO
.11
Gas T«i>.
CF)
rre
\
/
Gas Tenp.
CR)
Ts
Molecular
Nt.
«S
-
Velocity
(ft/see*
vs
Zi.f
J.H.t
2(.l
21.2
21.2
30.6
02
Cone.
(» Dry)
1
-
6003-13
668
-------
VELOCITY TRAVERSE
Prolectt Test Description!
Datet
location! 12- Stack Cross Section
Oniti / . .
Test! Personnel:
Pueli
Barometric Press, (in. Bg)i
Absolute Static Press, in Stack (in. Ha)i (P.) " <
Pitot Tube Coefficient: (C.)
[T APT1'2 - - - - - -------
•£L^^ I
SB J ::..::::::::
j. e — 5 f • .--...
f^ 3 ^ ' $ •.••„•...
Ti«e
Traverse Point
Port Depth
#3
1
17
vr
*3
1
27
1?
63
q
-27
yr
43
Velocity
Bead
(in. H,0)
iP
.*e
.0?
.0*
.01
.01
.Of
.03
.0(
.01
.03
0
0
Gas leap.
m
IH7Z
Gas Tenp.
(•R>
*S
Molecular
Mt.
«S
-
Velocity
(ft/sed
VS
31,2.
V-7
It, 2
12,7
I*-?
J>.2~
zz-t
If.*
12*7
H.l
0
0
02
Cone.
(% Dry)
2.2. .
6002-13
669
-------
Date /f OCT.
K V B. INC.
Test Mo.
TEST
UNIT NO.
SOx DATA SHEET
_ FUEL jjK &4* LOAD fclb/hr location
Box No.
Time
K
Temp, in Gas Meter
Press, in Gas Meter
Meter Reading
Barom. Press.
Percent Oxygen
K2 Purge Time
/
01* /
?e
0
6
*9.!*
2./
Ots 3
/
09-rt?
fQ
O
/.*+(>
Jf.g*
3./
/
60-14
sox
6 70
-------
Date /?
K V B. INC.
Test
SOx DATA SHEET
TEST
UNIT NO.
FUEL t.f.61*10*0 JObThr • Location /*•
Box No.
Tine
Temp, in Gas Meter
Press, in Gas Meter
Meter Reading
Barom. Press.
Percent Oxygen
Nj Purge Time
J
/OC?
s-o
0
&
xt.t*
/9JL I
^
/OJtiT
fJt
C
J.OOO
*?.**-
/Oft
(A "
Calculation: S03 or S02, ppm -
Exce» 02 %
A•• Ml of lead perchlorate used for sample •
B « Ml of lead perchlorate used for bland •
N • Normality of lead perchlorate titrant -
F • Dilution factor •
T • Average temp, in gas meter »
V • Volume of gas •ample ft? • •
P •> Barometric pressure •
p • Pressure in gas meter •
Concentration,C, ppm m
x 24
whan
Emiition-«E> g/Mcal
Ib/NBtu
ng/3
C • pollutant concentration, g/dsco .
», volu»« factor • dicn/10 oal
f*OB *od. Xeg. 9/11/74 p 32856
so2
/f.3
2./
.6/71
SC
jr//
S,»66
Sit*
0
/£*
so3
XAk-
8./
.0/7?
/
J-//
s,ecf
*1. to.
0
Jlif
s°x
60-14
wv. i/2/73
67 1
-------
Date 19 OG.T *7(»
K V B. INC.
Test
SOx DATA SHEET
TEST NO
.»/*-'
UNIT NO.
FUEL X.
LOAD
Jclb/hr
Location
Box No.
Time
Temp, in Gas Meter
Press, in Gas Meter
Meter Reading
Barom. Press.
Percent Oxygen
N2 Purge Time
/
/63&
??
O
o
JW.**
3.7
//oo
/
/Oft
*V
O
//6-60
.29.**-
3,7
//JO
Calculation: S03 or 80^ ppm = (A- B) «H «Fg U60 * T) x 24
Excess 02 3.7 %
A•« Ml of lead perchlorate used for sample = /O. 0
B B Ml of lead perchlorate used for bland
N » Normality of lead perchlorate titrant
F •> Dilution factor
T ° Average temp, in gas meter
V * Volume of gas sample ft3
P ** Barometric pressure
p ** Pressure in gas meter
Concentration, C/ ppm
B - CtT 2090 1
bo.S-XQj I
•where L J
Emission -,E, g/Mcal - .
Ib/MBtu "
ng/J -
so2
/O. 0
?./
. 0/7?
>o
J-/O
A««o
*?.*«
d>
/•/o
so3
//. 0
I.I
,e/?9
/
jr/o
/.Ot>0
2l,t*
0
2/
sox
•
C " pollutant concentration, g/dson .
F. volume factor - dscm/10 cal
from Fed. Reg. 9/11/74 p 32656
60-14
rev. 1/2/75
672
-------
TABLE .. TRACE SPECIES AND ORGANICS SAMPLING' CONDITIONS
PETROLEUM PROCESS HEATER - LOCATION 12/2
TS&O Run No.
Test No.
Date
Port Location
Velocity, m/s (f/s)
Stack Temp. , K (°F)
Oxygen Content, % dry
Moisture, %
Sample time, min.
Cyclone Flow, awcrran (awcfm)
, Isokinetic Rate, %
Oven Temp. , K (°F)
XAD-2 Temp., K (°F)
Meter Temp., K (°F)
Nozzle Size, mm (in.)
No. Filters Used
Sample Flow, Dry, scmm (scfm)
Volume Collected, Dry, scm (scf)
Particulate weight, g
Solid Particulates, ng/J (lb/10 Btu)
Stack Flow Rate, Nm /s (scfm)
1
12/2-3
10/17/76
-------
KVB, INC, TRACE SPECIES AND ORGANICS SAMPLING DATA
ftertfff*
CD
Project!
Date i i
Location!
Oniti
£M M4$£ 3L 5A$* Personnel i M6£ArY #£WM& Barometric Press*
(o/sg/re
i* < •
F/LTf/t.
Probe Nocele Diameter (inches) i '16
2.77
(Dn)
Test! 12- /2-- 3 Absolute Static Press, in Stack (in. Hq) i (Ps)
Puali RfS; GAS Pi tot Tube Coefficient!
TIME
Real
1300
.1*30
Ht>0
liffS"
HO*
I1Z7
1537
Ho 7
tu? ..
I707
17*7
If 07
Elapsed
o
30
f0
/5"
r
17
57
51
?7
f?
ry
• p )
Oven
31 1
3?g
3?f
371
31(
317
^ . i •• '
1»5
1"2. ',
102-
101
319
Meter
In/Out
ff
7f
ff
£1
f2
\?3
r?
ft
n
f*.
ft
n
11
fo
f-3
60
€2.
?3
f2.
n
?3
r/
f*
Yg
Cone.
% dry
KVB 6002-12
-------
KVB, INC. TRACE SPECIES AND ORGANics SAMPLING DATA
Projects '
Dates
Locations
Units
Tests
Fuels /
rx£$- rxAftf
l*/*o/7£
I2\ <
12/x-f
?£S. GAS
Personnels BueHiHG HlUHtHG Barometric Press i 2
Probe Nozzle Diameter (inches) s
Absolute Static Press, in Stack (in. Hq) s ~.£?
Pitot Tube Coefficients
1.5~2.
(Dn)
(Ps)
(Cp)
TIME
Real
///$-
//V5~
121?
111?
I3lf
IM?
nir.to
if/1
Hit
i?/ £>t
1.0
l.^
1.0
1.*
1.0
l.f
Cum.
Meter
Volume
(ft3)
'/ff.ff2
2l).fOo
2ff.?eo
y oo. coo
312.300
Wf.tOO
'ff/l
£0}
Probe
f07
H&
iff
151
f}0
in
103
1?7
13*
tsr
y//
131
XAD-2
/*
fr
tr
70
0
1<>1
lof
W
101
too
103
lot
Meter
In/Out
ft
73
?*
rs
<3.
f}
tl
$r
tt
r?
go
73
Y*
Vf
Tl
iTJ
7*
63
-•
£2
Ti
T7
&
5V
F8
°2
Cone.
% dry
nm «nn->_i7
CD
-------
TRACE SPECIES AND ORGANICS TEST
SAMPLE RECOVERY XXX!
Test No. 12./&-3 Date \ O- 1 grlfa location lZ
Sample Port Position &5TXg.£ — V\o
- Q*g» V.JseL-
Data Sheet KVB 6002-15
676
-------
12-Petroleum Process Heater
Test 12/2-3
TABLE
Stack - no collector - gas fue
POLLUTANT
SAMPLE NUMBER
Antimony
Arsenic
Barium
Beryllium
Cadmium
Calcium
Chromium
Cobalt
Copper
Iron
Lead
Manganese
Mercury•
Nickel
Selenium
tellurium
Tin
Titanium
Vanadium
Zinc
Chloride
Fluoride
Nitrates
Sulfates
277*
S2.0
O.OS
o.n
o.os
0.08
tu.o
<0.03
S
-------
12 - Petroleum Process Heater
Test 12/2-3 TABLE stack - no collector-gas fuel
POLLUTANT SAMPLE NUMBER
Antimony
Arsenic
Barium
Beryllium
Cadmium
Calcium
Chromium
Cobalt
Copper
Iron
Lead
Manganese
Mercury
Nickel
Selenium
Tellurium
Tin
Titanium
Vanadium
Zinc
Chloride
Fluoride
Nitrates
Sulfates
375*
<-o.oi
rt».OOS
-------
TRACE SPECIES AND ORGANICS TEST
SAMPLE RECOVERY LOG
f
Test No. 12/g-t. Date l6-2O-7<. location |Z-r$&reexje.ti
Sanple Port Position
.U.
679
-------
Test No.
TRACE SPECIES AND ORGANICS TEST
SAMPLE RECOVERY LOG
Date to-Zo-7g» location * 2. -
SanipXe Port Position
Data Sheet KVB 6002-15
680
-------
12-Petroleum Process Heater
Test 12/2-6 TABLE Stack-no collector-gas fuel
POLLUTANT , SAMPLE NUMBER
Antimony
Arsenic
*
Barium
Beryllium
Cadmium
Calcium
Chromium
Cobalt
Copper
Iron
Lead
Manganese
Mercury
Nickel
Selenium
Tellurium
Tin
Titanium
Vanadium
Zinc
'Chloride
Fluoride
Nitrates
Sulfates
278+
' —
—
T-
—
— ,
—
—
.—
-^
-fp.2.
—
TT •
— '
—
—
. —
y?oc
(3<*O)
<7f/000
D*
.0«>S
O.OI
O-lo
0.2.1
-ro.os
O.02.
I.*!
4^o.o3
ZJ
«C0.0o5
0.8S
-s
0
F* dupl
*ro.s
4TO-0/O
<0-OS
^o*ooS
^D»0 1
0.08
o.os
o o S
o* / o
.
KM
Si3, $!«»•
SiS
68 1
-------
KVB Analysis Data ;
Test Sample Number POM's . PCB's
5 298 < 1 ug/g < 1
12/2-6 534 < 1 ug/g < 1
534 (duplicate) < 1 ug/g < 1 ug/g
13-18 740 90 ug/g '< 1 ug/g
13-18 282 49 ug/g < 1 ug/g
13-18 *30 3.2 ug/g; < 1 ug/g
13-18 1038 6.3 ug/g < 1 ug/g
13-18 1032 396 ug/g < 1 ug/g
13-18 1033 1 ug/g < 1 ug/g
13-18 1034 8 ug/g < 1 ug/g
13-18 1034 (duplicate) 9 ug/g < 1 ug/g
13-24 735 513 ug/g < 1 ug/g
531 6.9 ug/g < 1 ug/g
1039 20 ug/g < 1 ug/g
1035 144 ug/g < 1 ug/g
1036 10 ug/g < 1 ug/g
1037 7.1 ug/g < 1 ug/g
1037 (duplicate) 8.5 ug/g < 1 ug/g
14 556 70.5 ug/g < 1 ug/g
568 104 ug/g < 1 ug/g
532 10.7 ug/g < 1 ug/g
532 (duplicate)- 8.2 ug/g < 1 ug/g
15-10 1041 < 0.1 ug/g < 1 ug/g
1041 (duplicate) < 0.1 ug/g < 1 ug/g
. 1042 * *
15-11 941 < 1 ug/1 < 1 ug/1
1044 < 0.1 ug/g < 1 ug/g
1045 * *
19-1 LF * *
19-2 533 < 0.1 ug/g < 1 ug/g
533 (duplicate) < 0.1 ug/g <1 ug/g
C . <1 ug/1 v < 1 ug/1
C (duplicate) < 1 ug/1 < 1 ug/1
LF * *
*Sample extracts too concentrated to be able to determine an analytical value
. 682
-------
Reply to
COMMERCIAL TESTING & ENGINEERING CO.
etNMAl OFFICE*: tti NORTH LA SALIC STRICT, CHICAGO. ILLINOIS SOS01 • ARIA COOt III T1S-S4S4
• INStlUMINTAl ANAirSU DIVISION. I«US WUT 441M AVINUt COlOCN. CMOIADO IMOI. FMONtt
To: Mr. John 6. Mlchalovlc
Calspan Corporation
Post Office Box 235
Buffalo. NY 14221
P.O. No.: 27810
Sample No.: KVB 12/2-6 A 278
April 22. 1977
Analyst: S. Sweeney
IAD No.. 97-A197-134-31
CONCENTRATION IN PPM WEIGHT
ELEMENT
Uranium
Thorium
Bismuth
Lead
Thallium
Mercury
Gold
Platinum
Ir1d1um
Osm1 urn
Rhenium
Tungsten
Tantalum
Hafnium
Lutetian)
V
Ytterbium
Thulium
Erbium
Hoi ml urn
Dysprosium
CONC.
0.6
0.8
<0.1
6
0.2
NR
±0.3
•
0.3
NR - Not Reported
All elements not reported
Total wt. of filter
ELEMENT
Terbium
Gadolinium
Europium
Samarium
Neodyml urn
CONC.
0.1
0.1
<0.1
0.2
0.1
Praseodym1um<0.l
Cerium
Lanthanum
Barium
Cesium
Iodine
Tellurium
Antimony
Tin
Indium
Cadmium
Silver
Palladium
Rhodium
<0.1 ppm weight
was 0.7011 as
0.5
1
35
0.1
0.2
<0.3
0.3
4
STD
0.3
42
received.
ELEMENT
Ruthenium
Molybdenum
Niobium
Zirconium
Yttrium
Strontium
Rubidium
Bromine
Selenium
Arsenic
Germanium
Gallium
Z1nc
Copper
Nickel
Cobalt
Iron
Manganese
Chromium
Approved: JL
A 0.1457 gf
CONC.
0.5
<0.1
10
0.6
3
3
0.7
<0.2
2
<0.1
0.5
35
14
8
0.8
190
8
12
ELEMENT
Vanadium
Titanium
Scandium
Calcium
Potassium
Chlorine
Sulfur
Phosphorus
Silicon
Aluminum
Magnesium
Sodium
Fluorine
Oxygen
Nitrogen
Carbon
Bojron
Beryllium
Lithium
Hydrogen
Jf~^ . ^rf
CONC.
1
12
<0.1
MC
>500
150
MC .
23
MC
MC
MC
MC
-350
NR
NR
NR
150
<0.01
0.1
portf6n^asacra_ leached 1n ultra-
683
-------
Reply to
COMMERCIAL TESTING & ENGINEERING CO.
. acNiiAi orrictti til »O«TM LA IALIE titter. CMICAOO. ILLINOIS «o»oi • A*CA coot m »t»-«4»4
.'' INSIIUMfNIAl ANAIYM DIVISION. 1015 Witt 44TH AVCNUt OOlOfN. CtHOtAOO IMOI, PMONIi XM7W3JI
To: Hr. John Nlchalovlc
Calspan Corporation
Post Office Box 235
Buffalo, NY 14221
P. O. r*xi 27810
Sample No., 12/2 - 6 B II 534
Date: April 23, 1977
Analyit: s. Sweeney
IAD No., 97-A197-134-31
CONCENTRATION IN PPM WEIGHT
ELEMENT CONC.
Uranium 53
Thorium
Bismuth
Lead <2
Thallium
Mercury NR
Bold
Platinum
Irldlum
Osmium
Rhenium
Tungsten
Tantalum
Hafnium
Lutetlum
Ytterbium
Thulium
. Erbium
Holmlura
Dysprosium
ELEMENT CONC.
Terbium
Gadolinium
Europium
Samarium
Neodymlum
Praseodymium
Cerium
Lanthanum
Barium , 11
Cesium <0.1
Iodine 0.7
Tellurium
Antimony
Tin <0.9
Indium STD
Cadmium <0.7
Silver 10.4
Palladium
Rhodium
ELEMENT
Ruthenium
Molybdenum
Niobium
Zirconium
Yttrium
Strontium
Rubidium
Bromine
Selenium
Arsenic
Germanium
Gallium
Z1nc
Copper '
Nickel
Cobalt
Iron
Manganese
Chromium
CONC.
10
3
2
0.8
1
<0.7
<0.2
£0.3
3
2
2
0.1
24
0.6
3
ELEMENT
Vanadium
Titanium
Scandium
Calcium
Potassium
Chlorine
Sulfur
Phosphorus
Silicon
Aluminum
Magnesium
Sodium
Fluorine
Oxygen
Nitrogen
Carbon
Bqron
Beryllium
Lithium
Hydrogen
CONC.
0.2
4
<0.1
110
37
3
11
' 15
62
2
13
38
-11
NR
NR
NR
3
0.1
>'
NR - Not Reported
All element! not reported <0*4ppm weight.
Sample was thermally ashed 9 350 C for
_nrlflr.Jto.
Approved, //(.
one hour In a labora
furnace In a quartz crudb
684
-------
Reply to
COMMERCIAL TESTING & ENGINEERING CO.
GENUAL OFFICE*: tli MOUTH LA (ALL! (T*(IT, CMIC4OO, ILUNOII tOtOI • A«IA CODI tit Tf •-•414
INJttUMINtAl ANA1YSU OIVUION. 14115 Wilt 44TH AVfMUt. GOIMN. COICMADO «04»l. FHOWi MMIM91
To: Mr. John G. Mlchalovlc JblEiW
Calspan Corporation «~ —
Post Office Box 235
Buffalo, NY 14221
P.O. NOJ 27810
Sample No.. 12/2 - 6 B 12 534
; I
Date: April 23. 1977
Analytti S. Sweeney
IAD No.. 97-A197- 134-31
CONCENTRATION IN PPM WEIGHT
ELEMENT
Uranium
Thorium
Bismuth
Lead
Thallium
Mercury
Gold
Platinum
Irldlum
Osmium
Rhenium
Tungsten
Tantalum
Hafnium
Lutetjura
Ytterbium
Thulium
Erbium
Hoi ml urn
Dysprosium
CONC. ELEMENT CONC.
<3 Terbium
Gadolinium
Europium
<2 Samarium
Neodymlum •
NR Praseodymium
Cerium <0.5
Lanthanum <0.9
Barium 9
Cesium
Iodine 0.6
Tellurium <0.7
Antimony
Tin <0.8
Indium STD
Cadmium <0.5
Silver 2
Palladium
Rhodium
MR - Not Reported
All element! not reported <0.4 ppm weight^
.- Samole was thermally ashed 9 35ir C for
ELEMENT
Ruthenium
Molybdenum
Niobium
Zirconium
— Yttrium
Strontium
Rubidium
Bromine
Selenium
. Arsenic
Germanium
Gallium
Zinc
Copper
Nickel
Cobalt
Iron
Manganese
Chromium
Approved: J
one hour In aO
CONC.
4
1
0.5
0.1
<0.8
<0.2
<0.3
8
4
2
<0.1
14
0.4
2
aoordcopj
ELEMENT
Vanadium
Titanium
Scandium
Calcium
Potassium
Chlorine
Sulfur
Phosphorus
Silicon
Aluminum .
1
Magnesium
Sodium
Fluorine
Oxygen
Nitrogen
Carbon
Boron
Beryllium
Lithium
Hydrogen .
^fck , * , ^
f furnace In
CONC.
0.2
4
<0.1
57
46
5
23
29.
57
2
11
110
•13
NR
NR
NR
2
, 0.1
NR.
a quartz cruc
685
-------
Rr"'«to
COMMERCIAL TESTING & ENGINEERING CO.
CCNtlAL OFFICE!: tat MOUTH LA lAltE STREET, CHICAGO. ILLINOIS SDtOI • A«EA CODE III 71S-M14
INS1IUMIN1A1 ANAIYSIJ DIVISION. 14115 WIST «TH AVtHlUL, GOIDEN. COIO1ADO SMOI, PHONI, XOZ7S-WI1
xigrv
I* Mr. John G. Michalovic jgjB&L.
Calspan Corporation •—
Post Office Box 235
Buffalo; NY 14221
P.O:NO.S 27810
Sample No.: /.?/? -( £
•
ELEMENT CONC.
Uranium .< 3
Thorium
Bismuth
Lead ^ -2.
Tha-llium
til. try UR
Gold
Platinum
Iridium
Osmium
Rhenium
Tungsten
Tantalum
Hafnium
Lutetium
Ytterbium
Thulium
Er'-'um
I j
**~s
Holmium
Dysprosium
*7 * #2. • f-9tf
CONCENTRATION
ELEMENT CONC.
Terbium
Gadolinium
Europium
Samarium
Neodymium
Praseodymium
Cerium <.o.H5~
Lanthanum < o.fS"
Barium t O
Cesium ^ ..2.5"
lod.ne . A«T
Tellurium < 0.ff
Antimony
Tin
-------
COMMERCIAL TESTING & ENGINEERING CO.
•INIRAL OrriOIt! Ml NORTH LA SALLI STRUT, ONIOAOO, IlllNOIt IOIII • ARIA 0001 lit TII>MI«
INtmiMINTAl ANAlYdl OIVIUON, I4JM WUT 44TM AVINUI. OOIOIN, COIOIAOO IOMI. MONIi MMTMBI
Mr. John 6. M1chalov1c
Calspan Corporation
Post Office Box 235
Buffalo, New York 14221
P.O. No.: 27310
Sample No., KVB 12/2-6 C ; 343. 344, 345,
511. 512. 513. 514, 5!5.
D«t.> April 22, 1977
Analycti S. Sweeney
350. 352. 527, IAD No., 97-Al97-134-31
ELEMENT CONC.
Uranium £0.03
Thorium
Bismuth £0.007
Lead £0.02
Thallium
Mercury NR
Gold
Platinum
Iridium
Osmium
Rhenium
Tungsten
Tantalum
Hafnium
Lutetlum
Ytterbium
Thulium
Erbium
Hoi mi urn
Dysprosium
ELEMENT CONC.
Terbium
Gadolinium
Europium
Samarium
Neodymi urn
Praseodymium
Cerium 0.004
Lanthanum 0.009
Barium 0.1
Cesium <0.002
Iodine 0.006
Tellurium
Antimony <0.007 '
Tin
Indium STD
Cadmium <0.006
Silver 320
Palladium
Rhodium
ELEMENT
Ruthenium
Molybdenum
Niobium
, Zirconium
Yttrium
Strontium
Rubidium
Bromine
Selenium
Arsenic
Germanium
Gallium
Zinc
Copper
Nickel
Cobalt
Iron
Manganese
Chromium
CONC.
0.02
0.005
0.03
£0.001
0.01
£0.01
£0.002
0.2
0.04
0.06
0.003
0.2
0.009
0.02
ELEMENT
Vanadium
Titanium
Scandium
Calcium
Potassium
Chlorine
Sulfur
Phosphorus
Silicon
Aluminum
Magnesium
Sodium
Fluorine
Oxygen
Nitrogen
Carbon
Boron
Beryllium
Lithium
Hydrogen •
CONC.
0.001
0.04
£0.002
5
MC
0.2
MC
0.5
1
0.08
0.6
MC
«9.06
NR
NR
NR
0.004
.
0.005
NR
NR - Not Reported
All elements not reported <0.004 yg/ ml
Approved)
687
-------
Mr. S. C. Hunter -3-
KVB ANALYSIS DATA
SAMPLE POM'S PCB's
12/2 - 3 B
12/2 - 6 E
13/18 M
13/18 M deep
13/18 N
13/24 609
13/24 A
< 10 ug/1
10 ug/1
2480 ug/1
2890 ug/1
225 ug/1
234 ug/1
10 ug/1
< 1 ug/1
< 1 ug/1
< 10 ug/1
< 10 ug/1
< 10 ug/1
<• 10 ug/1
< 5 ug/1
14 616 27 ug/1 < 10 ug/1
12/2-3 B 374, 376, 377
12/2-6 E 343-345, 350
I
13/18 M 605, 606, 607, 333
13/18 N - 264, 331
13/24 A 476, 610, 608, 611, 482, 488, 494
688
-------
KVB Analysis Data
Test Sample Number POM's . PCB's
- 3 298 < 1 ug/g < 1 ug/g
12/2-6 534 < 1 ug/g < 1 ug/g
534 (duplicate) < 1 ug/g < 1 ug/g
13-18 740 90 ug/g < 1 ug/g
13-18 282 49 ug/g < 1 ug/g
13-18 *30 3.2 ug/g < 1 ug/g
13-18 1038 6.3 ug/g < 1 ug/g
13-18 1032 396 ug/g < 1 ug/g
13-18 1033 1 ug/g < 1 ug/g
13-18 1034 . 8 ug/g . < 1 ug/g
13-18 1034 (duplicate) 9 ug/g < 1 ug/g
13-24 735 513 ug/g < 1 ug/g
531 6.9 ug/g < 1 ug/g
1039 20 ug/g < 1 ug/g
1035 144 ug/g < 1 ug/g
1036 10 ug/g < 1 ug/g
1037 7.1 ug/g < 1 ug/g
1037 (duplicate) 8.5 ug/g < 1 ug/g
14 556 70.5 ug/g < 1 ug/g
568 104 ug/g < 1 ug/g
532 10.7 ug/g < 1 ug/g
532 (duplicate) 8.2 ug/g < 1 ug/g
15-10 1041 <0.1 ug/g <1 ug/g
1041 (duplicate) < 0.1 ug/g < 1 ug/g
1042 * * •
15-11 941 < 1 ug/1 < 1 ug/1
1044 <0.1 ug/g <1 ug/g
1045 * . • • *
19-1 LF * *
19-2 533 <0.1 ug/g < 1 ug/g
533 (duplicate) <0.1 ug/g <1 ug/g
C < 1 ug/1 < 1 ug/1
C (duplicate) < 1 ug/1 < 1 ug/1
LF * *
*Sample extracts too concentrated to be able to determine an analytical value.
689
-------
WOOD-BARK BOILER
Location No. ' O . Unit No,
Unit Description (jJoQb - ~5b
45,4-00 VJfa-(l 00/ 000
Installation Date
Heater Rating
Burner Description
Test Fuel Combinations
Fuel Temp, at Burner (°F)
Primary Air Temp. (°F)
Comments:
690
-------
Test Mo.
Btoit Mo.
MOBILE lABORXTOM MIA
Date //-«g-7fe Location /J
Test No.
Engr.
Capacity
. OOP
Unit Type U/c£~rX.O/T
1. Test No.
2. Date
3. Tine
4. load (jk/#t. S7%**Y
5. Process Rate
6. Flue Diam. or Size, ft
7. Probe Position
B. Oxygen (%)
9. HOx (hot) read/3% 02 (ppm)
10. NO (hot) read/3% 02 (ppm)
11. M05 (hot) read/3% 02 (ppm)
12. NO (cold) read/3% 02 (ppm)
13. Carbon Dioxide (%)
L4. Carbon Monoxide (ppm) uncor/cor
15. Hydrocarbon (ppm) uncor/cor
16. Sulfur Dioxide (ppm) uncor/cor
17. Smoke Spot (Bacharach)
1 0 .JLfcJLia Tfrmii f *V /ABB
^O« ^mMD^^^^wWI^r I C /i^^Bi
19. Dew Point Temp. , (°F/m)
20. Atmos. Pressure (in. Hg)
21. Relative Humidity (%)
22.
23.
24.
25.
26.
27.
28.
29.
30.
73- /
U-X-7L
0\V2
93K
—
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7.7
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6 go
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7
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$ ^
Data Sheet 6002-2
69 1
-------
Test Mo. /3
Quit MO. y
Date
NOBILB LABORATORY DATA
Location
Test No..
Bngr.
Capacity
S0O. e>oo
Unit Type
(J.T.
Burner Type SfT/ea /r
1. Test No.
2. Date
3. Tine
4. Load (iL /&• ST£*/»\
\ ^
5. Process Rate
6. Flue Diam. or Site, ft
7. Probe Position
8. Oxygen (%)
9. NOx (hot) read/3% 0: (ppm)
10. NO (hot) read/3% 02 (PPB)
11. NO? (hot) read/3% 02 (ppm)
12. NO (cold) read/3% 02 (ppm)
13. Carbon Dioxide (%)
14. Carbon Monoxide (ppm) uncor/cor
15. Hydrocarbon (ppm) uncor/cor
16. Sulfur Dioxide (ppm) uncor/cor
17. Smoke Spot (Bacharach)
18. Ataos. Temp. (*?/•*>
19. Dew Point Temp. (*F/M
20. Ataaos. Pressure (in. Hg)
21. Relative Humidity (%)
22.
23.
24.
25.
26.
27.
28.
29.
30.
J3- I
//-«- 74
0900
97000
—
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3
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ta.
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as/
aaf
/&
310
— •'
I?
0
800
£(.
O
/t>91
—
3t
30
39. ti,"
#9
^
^
N
> "iu
4 %
1> «>ft
Data Sheet 6002-2
692
-------
MOBILE LABORATORY DATA
Test No. M'3 Date //-V-7& Location
Unit No. ff Fuel &**. »
Test No._
Bngr. B'
Capacity
. OOP
nnit Type 6t)/C<*
Burner Type
*TC /<"£"<.
1. Test Mo.
2. Date
3. Tine
4. Load
5. Process Rate
6. Flue Dian. or Size, ft
7. Probe Position
8. Oxygen (%)
9. MOx (hot) read/3% O? (ppm)
10. NO (hot) read/3% 02 (ppn)
11. NOa (hot) read/3% Oj (ppn)
12. NO (cold) read/3% 02 (ppn)
13. Carbon Dioxide (%)
14.- Carbon Monoxide (ppn) uncor/cor
15. Hydrocarbon (ppm) uncor/cor
16. Sulfur Dioxide (ppn) uncor/cor
17. Smoke Spot (Bacharach)
10. /tmoj^ltiL ff^'C)
19. Daw Point Temp. C/iV0C)
20. Atmos. Pressure (in. Bg)
21. Relative Humidity (%)
22.
23.
24.
25.
26.
27.
28.
29.
30.
/S-9
JJ-V-7L
0333-
9/tt>oo
«• •
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III
a.
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-------
Test Mo. /3-3
Btait Mo. f
MOBILE LABORATORY DMA
Date H-¥-7b location S3
Test Ho. /3-3
Engr./l
Onit Type_
fuel &W +6**K- Capacity
id* 77
Burner Type DSTfjO/T
1. Test Mo.
2. Data
3. Tine
4. Load tks/)f
5. Process Rate
6. Flue Diam. or Size, ft
7. Probe Position
8. Oxygen (%)
9. NOx (hot) read/3% Oa (ppm)
10. NO (hot) read/3% 02 (ppn)
11. NOa, (hot) read/3% 02 (ppm)
12. NO (cold) read/3% 02 (PPm)
13. Carbon Dioxide (%)
14. Carbon Monoxide (ppm) uncor/cor
15. Hydrocarbon (ppm) uncor/cor
16. Sulfur Dioxide (ppm) uncor/cor
17. Smoke Spot (Bacharach)
18 n^yr *££* j^">o
u>er- 0«*& .Xv«
20. Atmos. Pressure (in. Hg)
21. Relative Humidity (%)
22.
23.
24.
25.
26.
27.
28.
29.
30.
/j./y
//-V-7*
/¥*.*-
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Data Sheet 6002-2
694
-------
Test Mo. /3
Chit Mo.
Date >/-
MOBILE LABORATORY DATA
-76 Location _ ,/JL
teat Ho.
capacity
Unit Type_
t4>>7T
Burner Type X>ETK. C/T JS Tg
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gjr
CfMTFX.
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Data Sheet 6002-2
695
-------
Test Mo.
unit Mo.
MOBILE LABORATORY DATA
Date S/-/6-7& Location /
Fuel
Teat Mo.
. Engr.
Capacity SOP K
Unit Type i*)ie.K.££ u)-T*
Burner Type
1. Tpst Mo.
2. Date
3. Time
4. Load (/O* liAr *7£**r)
5. Process Rate
6. Flue Diam. or Size, ft
7. Probe Position
8. Oxygen (%)
9. NOx (hot) read/3% 02 (ppm)
10. NO (hot) read/3% 02 (ppm)
11. NO? (hot) read/3% 02 (ppm)
12. NO (cold) read/3% 02 (ppm)
13. Carbon Dioxide (%)
14. Carbon Monoxide (ppm) uncor/cor
IS. Hydrocarbon (ppm) uncor/cor
16. Sulfur Dioxide (ppm) uncor/cor
17. Smoke Spot (Bacharach)
18. Atoos. Temp. t^fC.)
19. Dew 'Point Temp. /rfj°C)
20. Atmos. Pressure (in. Hg)
21. Relative Humidity (%)
22.
23.
24.
25.
26.
27.
28.
29.
30.
a- /I
//-se>-?t
OS-fO
87
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Data Sheet 6002-2
606
-------
Mat Ho._
onit Mo.
Pate
HDBIUC UkBOMUOIff DM*
-7l__ location /-3
TWt Ho._
. Bngr.
Capacity
Shit type <&/«.*.££. t>J,
Burner Type "&&TAO'
tSTO ice*
tfest Ho.
S3-/9
73-Jta
Date
.3t
jjk
5..
It
T..
li
9..
10.
ill
12.
13..
14.
i§i
16^
i2t
18.
19.
20.
21.
22.
23.
24.
25.
16.
27.
28.
29.
30.
S3&0
load
9*
Process Rate
Flue Diam. or Size, ft
Probe Position
Oxyqen (%)
HOx (hot) read/3% O2 (ppm)
t33
iff
**
-------
Test Mo..
Unit No.
MOBILE LABORATORY DATA
Date // -//'7L Location
Fuel
Test Ho._
. Bngr.
, Capacity.
Unit Type
lJ.77
Burner Type
1. Test No.
2. Date
3. Tine
4. Load
5. Process Rate
6. Flue Diam. or Size, tt
7. Probe Position
8. Oxygen (%)
9. HOx (hot) read/3% 02 (PPm)
10. HO (hot) read/3% 02 (P?n)
11. N05 (hot) read/3% 02 (PPm)
12. HO (cold) read/3% 02 (ppm)
13. Carbon Dioxide (%)
14. Carbon Monoxide (ppm) uncor/cor
IS. Hydrocarbon (ppm) uncor/cor
16. Sulfur Dioxide (ppn) uncor/cor
17. Smoke Spot (Bacharach)
18. Atnos. Temp. l*F>*C)
19. Dew Point Tenp. (°F/*C)
20. Atxos. Pressure (in. Eg)
21. Relative Humidity (%)
22.
23.
24.
25.
26.
27.
28.
29.
30.
/3-ai
J/-/S-7L
/OOO
gt.ooo
£t*rrr*.
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173
f
/9-f
fS&
aft
&
£97
/SO
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7*0
*?9
0
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,
*
-------
OPERATING DATA
Location 13
Test
Date
Time
Steam Flow. lb«/hr
Air Flow _
Steam Temp. , *F
F.W. Flow (lbs/hr)/F.W. Temp. (»F)
Air Temp, entering A.H. , *F
Air Temp, leaving A.H:, *F
Gas Temp, leaving Blr, *F
Gas Temp, leaving A.H.', °F
F.W. Pressure, psig
Steam Header Pressure, psig
S.H. Metal Temp., "F
F.D. Fan Press., in. H.,0
A.H. Outlet Press., in. H.O
Plenum Press., in. H_0
Over fire Air Press. , in. H_O
Furnace Draft, in. HO
Boiler Outlet Draft, in. H_O
A.H. Outlet Draft, in. H.O
Classifier Outlet, in. H,0
Dust Collector Outlet, in. HO
I.D. Fan Inlet, in. H.O
Bark Distribution Air, in. H.,0
East Grate Temp. , *F
West Grate Temp. , °F
Bark Screw (% max. RPM)
Overfire Air Damper % Open
Excess Air Setpoint
Furnace Draft Setpoint
Stoker Rotor Contr. Setpoint
Steam Flow Integrator,
U>s/hr x 125000
Opacity, %
Grate Speed (indie.)
/3//
//-ft -7 6
6***"
9391*0
93ooo
770
?**><> | Ufa
61
4/0
fsoo\ar*
60
39 y*
fSO
400
/o9o
600
79*
*.<•
*.£>
.9
/9.0
-./
-/./
-/.9 '•
-Jt.o '
-6.7
~/6.0
17.*'
4*>o
3 if
0
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49
f/
7*
171 yr*
30
4S
J2-4
//-X-7C.
fSSO
fl 9 QQ &
f 4 Q 0 O
790
//»/«•"( Jtf*
70
4*/
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too
797
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-/.
9fe>eo
91/000
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-6.4
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400
39*"
£/
/OO
49
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73
'736*1*1
34"
y«
*
699
-------
OPERATING DATA
Location 13
Test
Date
Time
Steam Flow, Ibs/hr
Air Flow a
Steam Temp. , *F
F.W. Flow (Ibs/hr) /F.W. Temp. (°F)
Air Temp, entering A.H. , °F
Air Temp, leaving A.M., °F
Gas Temp, leaving Blr, °F
Gas Temp, leaving A.H. , CF
F.W. Pressure, psig
Steam Header Pressure, psig
S.H. Metal Temp., °F
F.D. Fan Press., in. H.O
A.H. Outlet Press., in. H.O
Plenum Press., in. H_O
Overfire Air Press., in. H^O
Furnace Draft, in. H.O
Boiler Outlet Draft, in. H.O
A.H. Outlet Draft, in. H.O
Classifier Outlet, in. H.O
Dust Collector Outlet, in. H.O
I.D. Fan Inlet, in. H.O
Bark Distribution Air, in. H.O
East Grate Temp. , *F
West Grate Temp., °F
Bark Screw (% max. RPM)
Overfire Air Damper % Open
Excess Air Setpoint
Furnace Dr^ft Setpoint
Stoker Rotor Contr. Setpoint
Steam Flow Integrator,
Ibs/hr x 12500
Opacity, %
Grate Speed (indie.)
13*6
//-*-7&
oio-r
97,000
98,000
73f
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-------
Test
Date
Time
Steam Flow, Ibs/hr
Air Flow
Steam Temp., *F
F.W. Flow (lbs/hr)/F.W. Temp. (°F)
Air Temp, entering A.H., »F
Air Temp, leaving A.H. , *F
Gas Temp, leaving Blr, °F
Gas Temp, leaving A.H. , °F
F.W. Pressure, psig
Steam, Header Pressure, psig
S.H. Metal Temp., °F
F.D. Fan Press., in. H.,0
A.H. Outlet Press., in. B_O
Plenum Press., in, H_O
Overfire Air Press., in. H.,0
Furnace Draft, in. HO
Boiler Outlet Draft, in. H.,0
A.H. Outlet Draft, in. HO .
Classifier Outlet, in. H.,0
Dust Collector Outlet, in. H»0
I.D. Fan Inlet, in. H.,0
Bark Distribution Air, in. H..O
East Grate Temp., °F
West Grate Temp., °F
Bark Screw (% max. RPM)
Overfire Air Damper % Open
Excess Air Setpoint
Furnace Draft Setpoint
Stoker Rotor Contr. Setpoint
Steam Flow Integrator,
Ibs/hr x 12500
Opacity, %
Grate Speed (indie.)
OPERATINt
Locatioi
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-------
OPERATING DATA
location 13
Test
Date
Time
Steam Flow, Ibs/hr
Air Flow t
Steam Temp. , *F
F.W. Flow (lbs/hr)/F.W. Temp. ("F)
Air Temp, entering A.H. , °F
Air Temp, leaving A.H. , *F
Gas Temp, leaving Blr, °F
Gas Temp, leaving A.H., °F
F.W. Pressure, psig
Steam Header Pressure, psig
S.H. Metal Temp., °F
F.D. Fan Press., in. H,0
A.H. Outlet Press., in. HO
Plenum Press., in. HO
Over fire Air Press., in. H.,0
Furnace Draft, in. H.O
Boiler Outlet Draft, in. H.,0
A.H. Outlet Draft, in. HO
Classifier Outlet, in. HO
Dust Collector Outlet, in. H_0
Z.D. Fan Inlet, in. H_O •
Bark Distribution Air, in. H,O
East Grate Temp., *f
West Grate Temp. , °F
Bark Screw (% max. RPM)
Overfire Air Damper % Open
Excess Air Setpoint
Furnace Dcpft Setpoint
Stoker Rotor Contr. Setpoint
Steaa Flow Integrator,
Itos/hr x 125000
Opacity, %
Grate Speed (indie.)
/ J-A4
ti-t-Tt.
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gf.ceo
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-------
OPERATING DATA
Location 13
Test
/3-m.i
Date
H-so-tC.
/too
Steam Flow., Ibs/hr
17.
W.ooo
Air Flow
13,090
9V
Steam Tamp., »F
74S
710
P.M. Plow (lba/hr)/F.M. Temp. (*F)
Air Temp, entering A.H., *P
•70
70
70
76
70
Air Temp, leaving A.H., *P
Gas Temp, leaving Blr, *P
S3 A"
Gas Temp, leaving A.H., °P
¥2.0
VV6
P.M. Pressure, psig
/090
Steam Header Pressure, psig
too
&60
660
S.H. Metal Temp.,~ *F
197
1/8
79?
t/o
P.P. Pan Press., in. H.O
/•a.
A.H. Outlet Press., in. H.O
J.S'
/.o
Plenum Press., in. H.O
.3
.V
Over fire Air Press., in. H.O
It
/8
it
Furnace Draft, in. H.O
-.3
-.3
-. J
-.3.2
-.33
Boiler Outlet Draft, in. H.O
-t.*
-/.a.
A.H. Outlet Draft, in. H.O
-*.*
Classifier Outlet, in. H.O
-a.a.
-jr.a
-a.a.
Dust Collector Outlet, in. B;O
-L.I
X.D. Pan Inlet, in. H.O
-to
-to
Bark Distribution Air, in. H.O
/*>'*'
East Grate Temp., *F
Meat Grate Temp., *P
Bark Screw (% max. RPM)
49
Overfire Air Damper % Open
/CO
/DO
/oo
Excess Air. Setpoint
bo
Furnace Draft Setpoint
ft,
Stoker Rotor Contr. Setpoint
te,
73
73
73
Steam Plow Integrator,
Ibs/hr x 125000
Opacity, %
39
s-o
3V
Crate Speed (indie.)
703
-------
OPERATING DATA
Location 13
Test
Date
Time
Steam Plow, Ibs/hr
Air Flow
Steam Temp., •?
F.W. Flow (lbs/hr)/F.W. Temp. (°F)
Air Temp, entering A.H., °F
Air Temp, leaving A.H. , "P
Gas Temp, leaving Blr, °F
Gas Tempj. leaving A.B. , °F
F.W. Pressure, psig
Steam Header Pressure, psig
S.H. Metal Temp., *F
P.O. Fan Press., in. H,O
A.B. Outlet Press., in. H,O
Plenum Press., in. HO
Over fire Air Press., in. H,O
Furnace Draft, in. H^O
Boiler Outlet Draft, in. H,O
A.B. Outlet Draft, in. H_0
Classifier Outlet, in. H,0
Dust Collector Outlet, in. B.O
Z.D. Pan Inlet, in. H,0
Bark Distribution Air, in. H,0
Bast Grate Temp. , *F
West Grate Temp., °P
Bark Screw (% max. RPH)
Overfire Air Damper % Open
Excess Air 'Setpoint
Furnace Draft Setpoint
Stoker Rotor Contr. Sctpoint
Steam Flow Integrator,
Ibs/hr x 125000
Opacity. %
Grate Speed (indie.)
/3-x*
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-------
LOCATION 13
ttoodbark Fuel and Bottom Ash Analyses
Voodbarfc Voodbark
SASS Test BASS Test
Test 13-18 (1032) 11-9-76 Teat 13-24 (10351 11-11-76
fxoxlmste Anelysis: As Received Dry As Received Dry
Moisture, t 60.91 — 51.71 ~
Volatile Matter. I 27.79 71.10 36.66 75.92
Ash, 1 3.05 7.80 1.85 3.84
Fixed Cerbon. I 8.25 21.10 9.78 20.24
Vltlmate Analysis:
Moisture. 1 60.91 — 51.71
Carbon, I 18.71 47.87 24.40, 50.53
Hydrogen. * 2.20 5.62 2.94 6.09
nitrogen, I 0.21 0.53 0.18 0.37
Sulfur, Z 0.08 0.21 0.03 0.07
Ash, 1 3.05 7.80 1.85 3.84
Oxygen, I 14.84 37.97 18.89 39.10
(by difference)
Best of Combustion:
Gross BTD/lb 3219 8234 4065 8418
Met BTD/lb 3015 7713 3793 7854
Bottom Ash Bottom Ash
Test 13-18 (1033) 11-9-76 Test 13-24 (1036) 11-11-76
SASS Test SASS Test
Cerbon, \ 6.04 2.08
Cross Best of Combustion,
BTU/lb 34 12 *
* Hot an experimental remit. Value vas calculated from the ratio of the two
carbon,essays and the BTD analysis of the. sample Barked "Test 13-18".
705
-------
LOCATION 13
Coal Fuel.Analyses
. Test 13-18 Test 13-24
; 11-09-76 11-11-76
Ultimate Analysis:
Carbon, 7. 66.93 64.42
Hydrogen, 7. 4.93 4.88
. Nitrogen, % 1.49 . 1.33
Sulfur, 7.. ' 2.47 2.80
Ash, 7. 7.66 8.32
Oxygen, 7. : 16.52 18.25
(by difference)
Proximate Analysis: '
- Moisture, 7. 7.35 7.50
Ash, 7.: 7.66. 8.32
. Volatile Matter, 7. 46.15 . 46.26
••: Fixed Carbon,: 7. 38.84 37.92
Heat of Combustion:
Gross BTU/lb 11,970 11,730
! Net BTU/lb 11,510 11,280
7.06
-------
Test No.
Unit NO.
PAKTICULATE EMISSION CALCULATIONS
Pate SS-M-7<» Location /3
Engr.
Sampling Train and Method
Pitot Factor, P»
Barometric Pressure, P.
Tot. Liquid Collected,
Velocity Bead. AP_».
>W./
bar
Particulate, M_
in. Hg
• gm
iwq Stack Temp., Ts 86 / *R Stack Area, As
ft
Sample Volume, Vm
Stack Press.,
_iwg Excess 02/ XO % f. V %
iwq Stack Gas Sp. Gravity, Gs
Orifice Press. Diff., H «
Sample Time, 6 9,t min Nozzle Dia., Dn
•1. Sample Gas Volume Vm^ - 0.0334 V"^-^ + H/13.6)
2. Water Vapor ^std * O-0474 vle
3. Moisture Content Bwo • Eq. 2/(Eq. 1 + Eq. 2)
n.d.
_in. Meter Temp., T
4. Concentration a. C - 6.0154 Mn/Vm
std
b. C - 2.205 x 10~6 Mn/Vm .
•to
c. C - Eq. 4b x 16.018 x 103
5. Abs. Stack Press, fa - P.. x 13.6 •*• Psg
SCF
SCF
grains/DSCF
6. Stack Gas Speed Vs - 174 Ps »®Ts x -0.
7. Stack Gas Plow a. Qsw - Eq. 6 x As x ^~ x ^~
Rate « 70-F Ts 40'
b. Qsd - Eq. 7a x (1. - Eq. 3)
8. Material Flow
9. XO factor
10. Emission
11. % Zsokinetic
Ms - Eq. 7b x Eq. 4b x 60
XO f • 2090/(20.9 - XO %)
a. E • Eq. 4b x Pe x Eq. 9
b. E - Eq. 4c x Pm x Eq. 9 x 1000
14077 x
/»./
qrams/DSCM
in. w abs.
ft/min
HSCF/min
DSCF/min
Ib/hr
N.D.
Ib/MMBtu
6 x Vs x Pa x Dn
/O3.72 ng/ joule
r %
Pe SC Feet/104 Btu
Fm SC Meters/104 joules
Oil
92.2
0.002475
Gas
87.4 ~
0.002346
Coal
.2
0.002636
•Multiply Vm(td by 530/T^CR) tf meter not temp, compensated.
Data Sheet 6002-4
707
-------
Test Ho.
Obit NO.
PARTICULATE EMISSION CALCULATIONS
Date //- 3*7& Location /3
Fuel A*& Ib/hr
N.D.
Ib/MMBtu
ng/joule
I -
14077 x T»(VmBt<1 + V
6 x Vs x Ps x On2
Fe SC Feet/104 Btu
Fm SC Meters/104 joules'
Oil
92.2
0.002475
Gas
87.4
0.002346
Coal
98.2
0.002636
•Multiply V»>td by 530/T^CH) if meter not texp. compensated.
fm « /OX. Off*
Data. Sheet 6002-4
708
-------
Test MO. X3-/7
Ohit Mo.
FARriCOLATE EMISSION CALCULATIONS
Date //->-76 Location >>_?
Fuel
Engr.
Pitot Factor, F«
.8V
Tot. Liquid Collected,
Velocity Head, 'AP .6
Sampling Train and Method
Barometric Pressure, P,
*«X./
la. Hg
/7/.J ml Total «M*MEii*e, "n_22*i2_"
iwg Stack Temp. , Ts f £ ? *R Stack Area, A
f t
Sample Volume, va
ftj
Stack Press., Pag •^•9f iwg Excess 0., *0-%_
Orifice Press. Diff., H >tfe jwg stack Gas Sp. Gravity, Gs
n.d.
Sample Time, Q 37 min Nozzle Dia., On Vx. ' in. Meter Temp., T
*1. Sample Gas Volume Vmatd - 0.0334 Vaffw^ + H/13.6)
2. Water Vapor Vw . . - 6.0474 V. '
»tQ 1C
3. Moisture Content Bwo - Eq. 2/CBq. 1 + Eq. 2)
4. Concentration a. C - 0.0154 Mn/Vm . _
Bta
b. C - 2.205 x 10~6 Mn/Vm
c. C " Eq. 4b x 16.018 x 10
5. Abs. Stack Press. Ps - P x 13.6 + Psg
6. Stack Gas Speed Vs • 174 Fs
SCF
SCF
N.D.
grains/DSCF
std
3
"
7. Stack Gas Flow a. Qsw • Eq. 6 x Ae x ^- x ^-.
Rate 6 70eF T8 40,
b. Qsd - Eq. 7a x (1. - Eq. 3)
grams/DSCM
". 63 in. w abs.
ft/min
WSCF/min
8. Material Flow
9. X02 factor
10. Emission
11. % Zsokinetic
Ms - Eq. 7b x Bq. 4b x 60
O>2f - 2090/(20.9 - J» %)
a. E - Eq. 4b x Fe x Eq. 9
b. E - Eq. 4c x Em x Bq. 9 x 1000
14077 x Ts (Vm ' -f Vta
I - 5
6 x Vs x Ps x On
JtSt 7 9f DSCF/min
3 Jf. 7 lb/hr
?7 N.D.
Ib/MMBtu
ng/joule
Fe SC Feet/104 Btu
Fm SC Meters/104 joules
Oil
92.2
0.002475
Gas
87.4
0.002346
Coal
98.2
0.002636
•Multiply Vm>td by 530/T^CR) if meter not temp, compensated.
6 A A*- S
f*. m S6J.1t
^, * ' .00
Data Sheet 6002-4
709
-------
Test No. X3-/7
Unit Ho. «3"
Pitot Factor, Fs
PARTICULATE EMISSION CALCULATIONS
Date S/-9-7& Location /3
Fuel fctf^fS Sampling Train and Method
Barometric Pressure, P.
Engr.
Tot. Liquid Collected, V
ml Total Particulate, M
_in. Hg
' M gm
Velocity, Head, AP . ^ / iwg Stack Temp. , Ts
*R stack Area, As f ?- 3J»"f t2
Sample Volume, Vm £Q ft Stack Press., Psg -«
iwg Excess 0 , XO % 6. 7^ \
Orifice Press. Diff., H . $(• iwg Stack Gas Sp. Gravity, Gs /_
n.d.
Sample Time, 687 min Nozzle Dia., Dn f/Jt in. Meter Temp., T
*1. Sample Gas Volume Vm - 0.0334 vm(P + H/13.6)
Vw . • - 0.0474 V.
std Ic
2. Water Vapor
3. Moisture Content Bwo - Eq. 2/(Eq. 1 + Eq. 2)
4. Concentration a. C - 0.0154 Mn/Vm _
std
b. C - 2.205 x lo"6 Mn/Vm
c. C - Eq. 4b x 16.018 x 10
std
3
5. Abs. Stack Press. Ps - P x 13.6 + Psg
6. Stack Gas Speed Vs - 174 Fs /APIs f~- x ~^-
vPs Gs
7. Stack Gas Flow a. Qsw - Eq. 6 x As x ~ x I6—
Fate 8 70-F TS 407
b. Qsd - Eq. 7a x (1. - Eq. 3)
8. Material Flow Ms • Eq. 7b x Eq. 4b x 60
9. XO2 factor XO f - 2090/(20.9 - K>2%)
10. Emission a. E - Eq. 4b x Fe x Eq. 9
11. % Xsokinetic
b. E - Eq. 4c x Fm x Eq. 9 x 1000
14077 x T»(Vm ..' + Vw ^)
I ^
8 x Vs x Ps x Dn
Fe SC Feet/104 Btu
Fm SC Meters/104 joules
Oil
92.2
0.002475
Gas
87.4
0.002346
Coal
98.2
0.002636
SCF
SCF
N.D.
~
. grains/DSCF
^
'_ Ib/DSCF
grams/DSCM
in. w abs.
ft/min
WSCF/min
DSCF/min
Ib/MMBtu
ng/joule
•Multiply Vmstd by. 530/T||(*IO if meter not temp, compensated.
Data Sheet 6002-4
7 I 0
-------
PARTICULATE EMISSION CALCULATIONS S/fS5
Test No. I3'lf Date /)/?/7& Location /3 Engr..
y I / . .
Unit No.
Fuel Coft//»-W Sampling Train and Method
____«« ]r -
Pitot Factor, Fs &• fc* Barometric Pressure, P. _#?. /F
ml Total Particulate, M
in. Hg
"
m gm
Tot. Liquid Collected, V
Velocity Head, AP ^^V iwg Stack Temp., Ts ?9/ "R Stack Area, As V 9.If ft2
Sample Volume, Vm 3ffi V ft3 Stack Press., Psg 'Glf iwg Excess 02, XO %
Orifice Press. Diff. , H /9. f iwg
7—
Sample Time, 6 ZWj min Nozzle Dia., Pn
Gs I.QVJ- n.d.
- - ^ ^
in. Meter Temp., T 5T/y
*1. Sample Gas Volume Vm - 0.0334 VB(P + H/13.6)
2. Water Vapor Vw • 0.0474 V.
sto ic
3. Moisture Content Bwo - Eq. 2/(Eq. 1 + Eq. 2)
std
4. Concentration a. C « 0.0154 Mn/Vm
b. C - 2.205 x 10"6
c. C - Eq. 4b x 16.018 x 10
5. Abs. Stack Press. Ps
std
3
Pbar x 13>6 + Psg
6. Stack Gas Speed Vs - 174 Fs i^PTs ~ x
7. Stack Gas Flow a. Qsw • Eq. 6 x As x f^ x ^r
Rate 6 70°F TS 40/
b. Qsd « Eq. 7a x (1. - Eq. 3)
8. Material Flow
9. X0_ factor
10. Emission
11. % Isokinetic
Ms
Eq. 7b x Eq. 4b x 60
X02f - 2090/(20.9 - X02%)
a. E - Eq. 4b x Fe x Eq. 9
b. E • Eq. 4c x Fm x Eq. 9 x 1000
14077 x Ts(Vm + Vw )
6 x Vs x Ps x Dn2
317./6 SCF
. /? SCF
K.D.
. &H>
grains/DSCF
. 6 g
0.0000/7;? lb/DSCF
O. a.7$"V grams/DSCM
in. w abs.
ft/min
WSCF/min
DSCF/min
lb/hr
. A.
Ib/MMBtu
ng/ joule
Fe SC Feet/104 Btu
Fm SC Meters/104 joules
Oil
92.2
0.002475
Gas
87.4
0.002346
Coal
98.2
0.002636
/0A-7?
0.1
•Multiply Vm td by 530/Tm(°R) if meter not temp, compensated.
Data Sheet 6002-4
7 1 1
-------
Test No. /3-2' ft
Sample Volume, Vm 37g--*" ft3 Stack Press., Psg -. .2 .if iwq Excess 0_, XO -*_JLl£L_*
Orifice Press. Dif f . , H
Sample Time
iwg Stack Gas Sp. Gravity, Gs /•6t/ n.d.
3OO min Nozzle Dia., Dn .
in. Meter Temp., T
/
*1. Sample Gas Volume Vm . _ = 0.0334 Vm(P. + H/13.6)
std bar
2. Water Vapor
std
0.0474 V
Ic
3. Moisture Content Bwo = Eq. 2/(Eq. 1 + Eq. 2)
4. Concentration a. C = 0.0154 Mn/Vm
std
b. C = 2.205 x lo"6 Mn/Vm
c. C = Eq. 4b x 16.018 x 10
std
3
5. Abs. Stack Press. Ps = P x 13.6 + Psg
.00
6. Stack Gas Speed Vs = 174 Fs /APTs - x
* VPs • Gs
7. Stack Gas Flow a. Qsw = Eq. 6 x As x f3-0- x 7^=-
Rate @ 70"F Ts 407
b. Qsd = Eq. 7a x (1. - Eq. 3)
8. Material Flow Ms = Eq. 7b x Eq. 4b x 60
9. XO factor
10. Emission
11. % Isokinetic
XO f = 2090/(20.9 - XO %)
a. E = Eq. 4b x Fe x Eq. 9
b. E o Eq. 4c x Fm x Eq. 9 x 1000
14077 x Ts (Vm " -f Vw )
_. std std
I =
6 x Vs. x Ps x Dn
Fe SC Feet/104 Btu
Fm SC Meters/104 joules
Oil
92.2
0.002475
Gas
87.4
0.002346
Coal
98.2
0.002636
3
SCF
SCF
N.D.
O. /^ 77 grains/DSCF
" lb/DSCF
0. S
2 3
>?«T.
grams/DSCM
in. w abs.
ft/min
WSCF/min
DSCF/min
Ib/hr
N.D.
Ib/MMBtu
ng/ joule
70.
'Multiply Vm ^, by 530/T (°R) if meter not ten?), compensated.
std m
Data Sheet 6002-4
7 1 2
-------
Test No..
Box No.
/3-7
Test Description
PARTICULATE CALCULATION SHEET
Date //-.3.-7£ location /3
Sample Probe Position Jo " s*i.
Test Crew
Dry Gas Hater Vol. (
Final /<£ *'• ?(.
Initial /& 01. 76-
Total £0 . O
Beaker No. 3
Date
Weighed //--2-7fc
Tare 1 /of. ?s/7
Wt. 2
3
4
5
6
Avq /o/. 12 f 7
Bottle No.
Impinger
Content (Water)
Rinse (ml) y-?f
Date Weighed
or 250 Bake //-.S--7C,
Final 1 /oa.soojT
Wt. 250 2 toa.seoV
3
4
5
6
Avg /a 3. ^ oo -J"
Residue wt .a/et
Final 250-Tare
Date Weighed
or 650 Bake
Final 1
Wt. 650 2
3
4
5
6
Avg
Residue Wt
Final 650-Tare
ftj)
]
/
/eo.o 97O
/oo.o<)7£>
.
/e>o .0 9 ?O
Probe
(Acetone)
ZOO
/CO . /» o 7
too .1*0-)
/e<3./j«7
iO 337
Final /(>
Initial /6
A Vol &
2
/e/.6ja&
st>/.6*ai>''
/o/. L *ar
Probe
(Water)
/J-0
/e/.4^8t
/DA &£Zb
/0/.£fg(.
.066 I
In
1
6 /
O /
6.
y
9?.af39
9».J«»
y.««l
eye
(Ace
3S<
>9. »'«"
91*j»o
W.a-ro*
.o/tl
ipinqer
2
^2
OO
3.3
HL°
£-
98. ^oV
?a. 9ao<^
??.9ao»
lone
tone)
/<£>£
9f.93o/
W.130I
M-too 1
.oe97
Water Vc
3
X-J'
o ;
s.*
(o
loa.im
/OO.Vrtj
Flask
(Dry)
/eo. ssif
/to.fuL
iot>.s»iL
leo.sail*
.OVW3
>1 (ml)
S. Gel 1
7*"7. 0
rvr.y
//•i x
Filter
No.
/O
. lO&,2
.Sola
• lots
/./C7J'
/. /07(.
/./0-?L
. 3o/f
total
°t't.
Blank
No.
//
.a*ef
. •Sft.S'
• loref
. 15-ff
. tegs-
• ISZS"
•&
Comments:
Data Sheet 6002-3
. po I
713
-------
Test No. X3-/7
Box No.
PARTICULATE CALCULATION SHEET
Date //-9-7t Location /3
Sample Probe Position
Test Crew
Test Description
Dry Gas Meter Vol. (ft**)
Final /?JJ. VJO
initial /*??. ^yo,o13 /
3
4
5
6
AVO IdO-D^'il
Bottle No.
Impinger
Content (Water)
Rinse (ml) £/0
Date Weighed
or 250 Bake //•/«• 76
Final 1 soG.ptri/y-
Wt. 250 2 IOG.3.WS-
3
4
5
6
Avg too.abtS-
Residue wt . /•>//
Final 250-Tare
Date Weighed
or 650 Bake
Final 1
Wt. 650 2
3
4
5
6
Avg
Residue Wt
Final 650-Tare
/£/. ^^ y_j
/ tf / tfeXVZ
ici, ifi^^>
Probe
(Acetone)
32 ±
/£/•£.*•*<_?
ltn.(,f^3
/»>: (*ft3
. 0900
9?.^y?9
99, ay?o
9 9.*^?o
Probe
(Water)
/ft^-
9f, J5"3Z
?9. 3X38
"
9f. ii"3Z
,<90V^
fr.f/J?
98. >/t1
^j.j/n
MO, mi
UO.V7J3
/eo.VSV
Cyclone
(Acetone)
y?i-
fg.13('
/• a<34
.VJd/
i
/7/.-S
Blank
NO.
. ?0 /^
. 80 //
. S 5 .'.•'
. go/o
'•4(0/0
, go / O
- . cwo/
'
Comments t
Data Sheet 6002-3
'* •
/t>0
* - .00' f^
71 4
-------
PLANT
LOCATION
OPERATOR
DATE
METHOD 5 CONTROL CONSOLE READINGS
/-3-?"
1
1
Stack .
Tempera-
ture
(Tg) »F
y/o
*/iSO
401'
Voo
31S
39*'
40
'
Velocity
Head
/. 76
/6/A^C
/^^/.oo
/£ 30.00
/CV0.60
/t>?9. oo
/66A76
Gas Sample
Temperature at
3ry Gas Meter
Inlet
(Tmin.)
«F
Outlet
(Tmout'
»P
^y
#0
yo
VO
-------
PLANT
METHOD 5 CONTROL CONSOLE READINGS
LOCATION /3
OP E RATOR_
DATE //-3-7S
RUN NO.
SAMPLE BOX NO.
METER BOX NO. '
4ETER H _ .~~
: FACTOR"!
AMBIENT TEMPERATURE
BAROMETRIC PRESSURE "
ASSUMED MOISTURE, % "
HEATER BOX SETTING "
PROBE LENGTH, IN.
NOZZLE DIAMETER, -Ml."
PROBE HEATER SETTING"
SCHEMATIC OF STACK CROSS SECTION
Traverse
Point
Number
40*"*'
TOTAL
kvroRrr
Sampling
Time
(e)Min.
/-s-o-sr
f**0
SS3^
-.,
Static
Pressure
.03JT
.osS
.03*'
-
Pressure
Differen-
tial Acres
Orifice
Meter
(AH),
In. H2O
* Q fa Q
1 & V @
.060
-
.
s Gas
Sample
Volume
(V ft\
/&&/.7L
S&70.00
M79.3/
Gas Sample
Temperature at
Dry Gas Meter
Inlet
(Tmin.)
op
Outlet
(T )
v mout1
op
#Q
yo-
yo
-
AVG.
nvr
Sample
Box
Temprta-
ture
*/f
*>#
d*
AVR.
Temperature
of Gas
Leaving
Condenser on
Jast Impinger
°F
9J"
ytr
y £ "*
1
\
1
1
i
]
•-
O>
-------
PLANT
LOCATION /3
OPERATOR
DATE //-8-7',J
TOTAL
WCRA^r
Sampling
Time
fc)tl»n .
d^Ofi-K.
T/tHs'
AT07
s&a.
J-s-37
j^^-2
;&£>7
S622
//"/T//*C_
-
Static
Pressure
)
Velocity
Head
.«v
,-oy
.oy
• oy
.°i
.<><{
,oV
•>,S
.8C,
/479.^^
s Gas
Sample
Volume
-------
PLANT
LOCATION /.3
OPERATOR
DATE //-"
CONSOLE READINGS
RUN NO. /3-/S
SAMPLE BOX NO.
METER BOX NO.
1ETER H ___
: FACTOR"!
AMBIENT TEMPERATURE
BAROMETRIC PRESSURE "
ASSUMED MOISTURE, % "
HEATER BOX SETTING "
PROBE LENGTH, IN. "
NOZZLE DIAMETER, IN."
PROBE HEATER SETTING"
SCHEMATIC OF STACK CROSS SECTION
Traverse
Point
Number
*0'/J
TOTAL
M*?T«* ^*»-
Sampling
Time
I . \ m | ,
•m^ffscstf.
dcoft*.
T/*>&
///-*""
HfS"
/a/*"
if-f^
,3,*r
I3S~O
/y/-»"
H*°
H^°
IfSL®
ty*r&
IffP-O
Static
Pressure
(Ps) ,
In. -Hg.
-
. - ->
Stack
Tempera-
ture
(Tg) °F
y^v
4^33
fzi
133
Cr
y^i-
y/7
y^?
ys/
Velocity
Head
(Ps}
• Of
,t>1
-oy
,0V
• ov
,oV
.oy
e& I>FS&
• oV
. oy
,o°
?&^-3«»0
oo I ,~?oo
Gas Sample
Temperature at
Dry Gas Meter
Inlet
(Tmin.)
op
VL
JT3
•TV
-S-i"
J-7
^2
J-7
i-H
-T4
JT6
5-7
Outlet
(Tmout>
°P
•f/
y?
jrO
J5-/
^y
-rr
j-^'' •
5-6
.rf
^y
JTf
AVG.
Sample
Box
remprta-
ture
Op -
371
rt>3
90s>"
(.
10 y
HOT
AVR.
Temperature
of Gas
Leaving
Condenser on
jast Impinger
OF
*3 '
s-*
*3
*-?
*~?
f3
trir
-------
>LAHT
^OCATION_.
OPERATOR
)ATE t/7"
«JN NO. xj
'.AMPLE BOX NO.
IETER BOX NO. "
IETER fl ' ~
; FACTOR"!
METHOD 5 CONTROL CONSOLE READINGS
AMBIENT TEMPERATURE
BAROMETRIC PRESSURE '
ASSUMED MOISTURE, % "
HEATER BOX SETTING "
PROBE LENGTH, .IN.
NOZZLE DIAMETER, IN."
PROBE HEATER SETTING"
SCHEMATIC OF STACK CROSS SECTION
•Traverse
Point
Number
TOTAL
Sampling
Time
f n \ lifi n
^^^^^^M»*
OLo&ie.
T/^f
/oVZ.
/Of7
///*
//«7
HS~?
/xsr?
/ayjz.
Static
Pressure
•/
.of
.01
.Q<{
,0*
.6*
Pressure
Differen-
tial Aero:
Orifice
Meter
(AH),
In. H2O
.0(0
f>
0
O
0
z>
o
s Gas
Sample
Volume
93-32
I7.l0
l-TWAl
/•?
-------
PLANT
LOCATION
OPERATOR
DATE
/7-x/-7AS~
to
•P
^8
33
57
?o
?o
43
*/
V*
V3
f(3
AVG .
AVG .
Sample
Box
Temprta-
ture
°P
399
?0^
-
AVR.
Temperature
of Gas
Leaving
:ondenser on
:.ast Impinger
op
Ab
n
ye
£-/
y
-------
Test No. /3-
CASCADE .IMPACTOR DATA SHEET
TEST RUN NO.
IMPACTOR NO.
LOCATION
DATE
/
CYCLONE NO.
OPERATOR
V "f
SAMPLE POINT LOCATION
SUBSTRATE COATING
FUEL
IMPACTOR ORIENTATION
FLUE STATIC PRESSURE
NOZZLE DIA. V
FLOW THRU IMPACTOR
"f- ^TEST LOAD -$0
kib/hr
CFM
inH?O, VELOCITY S3 ' •
"
mm IMPACTOR PRESSURE DROP
END TIME /•*"_? .3"
GAS METER END'
CF
GAS METER START
GAS VOLUME / /•
START TIME
DURATION
CF
FLOW RATE
CFM
AMBIENT TEMPERATURE 3*/
PRESSURE
IN Hg. HUMIDITY
FLUE GAS MOLECULAR WT. f
, TEMP .
F , DENSITY
g/cc, VISCOSITY
POISE
Foil + Sample, g
Unused Foil, g
Sample , g
Correction
for Blank, g
Final Sample , g
Stage Number
1
J.4^
3.t,s-ro
.00*3
.0022
2
S.aV-X*
3*W
00* <*
.OOZC,
3
3.LS*!
3.6*6*
.0039
.*>3
-------
TEST RUN NO.
IMPACTOR NO.
CASCADE IMPACTOR DATA SHEET
LOCATION
Test No. / 3-
DATE //- ? -
CYCLONE NO.
OPERATOR ,g.
SAMPLE POINT LOCATION
SUBSTRATE COATING -
0.6*14.
FUEL
TEST LOAD g O klb/hr
IMPACTOR ORIENTATION
FLOW THRU IMPACTOR
CFM
FLUE STATIC PRESSURE ___—..
NOZZLE DIA. 'f
_inH20,VELOCITY_
-f 4
mm IMPACTOR PRESSURE DROP
END TIME
GAS METER END /74|/?/'?
3. 7 «,-;/£>
.005A
— . .„
^
Stage
Blank
*J*
FILTER NO.
Sample Blank
FILTER + SAMPLE, g
FILTER TARE, g
SAMPLE, g
CORRECTION FOR
BLANK, g
FINAL SAMPLE, g
, */*y
,8/a7-
.aoy*
/Vrf
FULL CONTAINER, g _
EMPTY CONTAINER, g
CYCLONE CATCH, g
722
, *//
60-20
-------
TABLE 1.
Symbol Value
Pressure drop across impactor
during test "Hg" A?2
Static pressure at inlet to
impactor, atm.^ ?„
2
Dimension conversion constant
723
Density of aerosol particle, grams/cc P /• O
Density of gas at inlet sampling
conditions, grams/cc P
Molecular weight of sample gas • •MW 3&< /&
Molecular weight of calibration gas MW *
Temperature of gas at sampling
conditions, °K T 477
Temperature of gas at calibration
conditions, °K T ,
Static pressure under calibration
conditions, atm. P "
Gas viscosity at sampling conditions,
poises . y _J
Stage jet diameter, cm D
D 5 . 073X
CG —
Sample quantity collected on each cup R_
R3 .00
*4 ' 003
-------
TABLE 2.
Effective pressure drop, "Ho"
Inlet flow to impactor, cc/ second
Pressure out of stages, atm.
Density of gas out of the various
stages , grams/cc
Characteristic diameter, microns
Criteria for validity of equation 18
Mean free path
Average molecular velocity
Symbol Value
AP^ O . 3 V
?„ . 999
•j- • '
D *? ^ 9
_
P_3 .999
P? .997
p? . 992
"6
P., 7./X/«^
p~2 - . x -y
p- '' ' * /0
P^3 ?./t/G-?
"4 . S4
pc,
D 6 , -4
pc_ x 10
^6 _j- 7-7
T '
v ^.0^9//o^
Continued
724
-------
TABLE 2 (Continued)
Symbol Value
% on a cup of the total sample collected CYdOAtf .ooZO
Stage 2 Y .00 *A
; 5
6,;
Filter
*Any discrepancy due to rounding off should be buried
in the largest Y cumulative % smaller than D
pc
^2
725
3 v . *0*(.
Total "r'<9/:"ioO.OO*
Z5 H .1
-------
TABLE 1.
Pressure drop across impactor
during test "Hg"
Static pressure at inlet to
impactor , atm.
Density of aerosol particle, grams/cc
Density of gas at inlet sampling
conditions , grams/cc
Molecular weight of sample gas
Molecular weight of calibration gas
Temperature of gas at sampling
conditions, °K
Temperature of gas at calibration
conditions, °K
Static pressure under calibration
conditions, atm.
Gas viscosity at sampling conditions,
poises
Stage jet diameter, cm
Sample quantity collected on each cup
Dimension conversion constant
Symbol Value
AP,, 0.3~7
p, .99?
P /• & ~
P
^•5 ', 7f. ... ^\_™.. . •' '
2
MWm 3£>. /(o
2 ' """
MW, 2 8 < 9J"
i
2 •• •
•^ T , . . _ ,
j. —
P /
i.
y 3.VV/0~9
D . ^v?
o"2 .I7"7^
D"3 .13 9&
o"4 ,o9V6>
D^5 .073)
R^6 .0/2?
R , . 0/12
A
Q
i>
G "'-"',..
7 .._...
Q /
726
-------
TABLE 2.
Effective pressure drop, "Hg"
Inlet flow to impactor, cc/second
Pressure out of stages, atm.
Symbol
F
1
Value
O. r£7
/7..T
. 999
,999
.991
.99C,
.9*7
Density of gas out of the various
stages, grams/cc
Characteristic diameter, microns
Criteria for validity of equation 18
Mean free path
Average molecular velocity
pC
ic
4
L
V
Q . QGO 7f
6.
7.
7.QZ X
. 993
6..*.*!
/.
X so
Continued
727
-------
TABLE 2 (Continued)
Symbol
% on a cup of the total sample collected cy4AO*•<>
'•3
728
-------
PLUME OPACITY OBSERVATION RECORD
LOCATION NO.
OWNER
DATE //•3
OBSERVER
Test Run No._
. JSUE*>
BOILER NO. .5" CAPACITY /OO klb/hi
TYPE A#*K BURNER TYPE
POINT OF EMISSION
POINT OF OBSERVATION /g (S
»•*
TEST
No.
Tine
am/pm
Type
Test
Load
k#/hr
Opacity
HIND
Speed
tnph
Direct
Sky
Cond.
Sun
Posi
tion
Comments
//SO
90
// 59
il Yz
30
30
Si'
v,
30
S&03
30
3*
729
-------
PLUME OPACITY OBSERVATION RECORD
LOCATION HO.
OWNER
DATE _ //- ?-
/3
Teat Run No. S3- I 7
OBSERVER
CAPACITY
_ BOILER NO. A _
£M£ *
'.'FUEL TYPE £** !<. BURNER TYPE
klb/hi
POINT OF EMISSION
POINT OF OBSERVATION /CO
6> f*
NO.
TEST
Tine
am/pm
Type
Test
Load
k#/hr
Opacity
WIND
Speed
mph
Direct
Sky
Cond
Sun
Posi
tion
Comments
IfOO
•*• Xfl
to
At-
y
IS 31
O
ft
730
-------
VELOCITY TRAVERSE
TMt Description!
Datei
location!
Stack CTOM Section
l».t. Af -7
Personnel i
Barometric Press, (in. Bg)i
Absolute Static Presa. in Stack lin./sVrti —.3-iT (ff)
Mtot Tube Coefficieati . f ^
V, - 85.48
-
V.J
TiM
Travurs* Point
Fort Depth
'
l«
/*
/J
ay
so
36
fa.
vs-
Velocity
Bead
(in. B,0)
tf
,os
,o(»
,ot
.0*.
.of
.0*
, o»
.01
Gas Teap.
(•r)
'390
Gas T*qp.
CM
*S
Molecular
Nt.
"s
Velocity
(ft/see)
»S
Oj
Cone.
{* Dry)
6002-13
73 1
-------
too]act i
Date t //_
I/oca tlom_
Oniti
Teatt / 3
Fuel i
VELOCITY TRAVERSE
Tart Daacriptioni
Stack Croii Section
Personneli
B»ron«tric Presi. (In. 89)1
Absolut* Static Pr«i». in Stack (in. flT) i ~ • ^» *~
Pitot Tub* CoetficUnti . %¥
(P.)
•65-48
Tl»e
Travaric Poibt
Port Mpth
6"
/^*
/g^
^0*
*f"
30"
3L"
V*"
Velocity
Bead
(in. 8,0)
tf
O.SO
£>.0g
6.0V
.6VS
O. Oft*'"
e .09.
o.oi
O.oi
Ga* Tav
W
feX>
Caa Teap.
CR)
*S
8C,o
1
Molecular
Ht.
"S
Velocity
(ft/aaci
V8
Oj
Gone.
(% Dry)
•002-13
732
-------
Date
K V B. INC.
SOx DATA SHEET
NO.
f
TEST MO.
UNIT NO. s FUEL B*l*. LOAD $0 klb/hr location
Box No.
Time
Temp, in Gas Meter
Press, in Gas Meter
Meter Reading
Barom. Press.
Percent Oxygen
N2 Purge Time
/
X-?39
•S~9
O
0
*W1
8.JT
/*-S-S
/
S»J~/
•s-y
0
J,frOG
*
-------
Date /A ft - 74
KVB. INC.
Test No
. /3//
SOx DATA SHEET
/ ^r (J)ALlr
TEST N0.4&E UNIT NO. S FUEL ^^K. LOAD g<> Idb/hr Location X3
Box No.
Time
Temp, in Gas Meter
Press, in Gas Meter
Meter Reading .
Barom. Press.
Percent Oxygen
N2 Purge Time
.2
>339
4ry
0
O
.39.86
7.?
woo
2
/3JT3
-ry
£>
/,000
*<)*<*
7**'
SV**''
Calculation: SO, or S0_, ppm >
—> t<*
Excess O2 f'^ *
(A - B) x N x F x (460
V (P -f p)
T) x 24
A = Ml of lead perchlorate used for sample •=
B = Ml of lead perchlorate used for bland
N = Normality of lead perchlorate titrant
F = Dilution factor
T = Average temp, in gas meter
V - Volume of gas sample ft3
P = Barometric pressure
p = Pressure in gas meter
Concentration,C, ppm
,gm/dscm
Emission-,E, g/Mcal »
Ib/MBtu
ng/J -
- oT 2090 1
bo.s»-xo2 I
i«ra L J
E
where
so2
e / 7, O
C £ * /
,0096^
= X^
^-xf
e A«oo
^?-W
<5
?5^
B '
V
•
- .
so3
/A 9
L.f
. e>09±"
/
-5-xf
J.9QO
3<)A
-------
TABLE TRACE SPECIES AND ORGANICS SAMPLING CONDITIONS
LOCATION 13 - WOOD/BARK BOILER
TStO Run No;
Test NO.
Date
Port Location
Stack Velocity, n/s (f/s)
Stack Tesp., K (°F)
Oxygen Content, % dry
Moisture, %
Sample Time, min..
Cyclone Flow, awm /m (awcfm)
Isokinetic Rate, %
Oven Temperature, K (DF)
XAD-2 Temp., K (°F)
Meter Temp., K (*F)
Nozzle Sice, not (in.)
No. Filters Used
Sample Flow, dry, DNm /m (scfra)
Volume Collected, dry, DNm3(scf)
Particulate Weight, g ~
Solid Partieulates, ng/J (Ib/MMBtn)
13-18
11-9-76
Dust Coll. Outlet
4.42 (14.5)
495 (431)
8.4
9.6
300
0.065 (2.31)
93.5
429 (403)
291 (64)
285 (54)
19 (3/4)
1
0.372 (1.31)
11.25 (397.2)
3.0969
127 (0.296)
13-24
11-11-76
Dust Coll. Outlet
4.39 (14.4)
496 (433)
8.5
7.8
300
0.065. (2.31)
80.3
477 (398)
292 (65)
278 (41)
19 (3/4)
1
0.0371 (1.31)
11.17 (394.3)
3.2690
136 (0.316)
735
-------
TRACE SPECIES AND ORGANICS TEST
SAMPLE RECOVERY LOG
Test Mo. 13-18 Date V|-S7fa location lg>
Sample Port Position
Op"fert
t>i-r^.Toe.
— O»AJL.£.
T40
Container
Number
B32.
737
S30
wa.
sis
340
342.
\os4-
Saiq>le Description
"P + >4 -
SB
kfi_
«*=
Container
Type
S -
L-i
lfi-2.
Net
wt/vol.
0.2^47
3S4.il • -i
«
144. *(
Comment
4I7.S-275)
*9
Data Sheet KVB 6002-15
I<3C
736
-------
TRACE SPECIES AND ORGANICS TEST
SAMPLE RECOVERY LOG
Test
Mo. B-1 & Date
Location J3>
Sanple Port Position
Op 4lfeci?> -Cci
ftA_£ U
15-18 E.
IS-*
I2H8P
&H U
Srfi 1C
Container
Number
4^2-
Bib
517
;-MG» 4zo
Sanple Description
(S) A /i
IMP * 1
4-2
SB
»-6>
M.P
SP
S- '4
SB-
SC- 2.
1C> &OLI&&
Container
Type
CAK!
L-l
Net
*rt/vol.
204-
Comment
J_
£.4%
Data Sheet KVB 6002-15
737
-------
13 - Wood Bark Boiler
Test 13-18 . . . TABLE Downstream of Precip.-coal 8. wood f
POLLUTANT SAMPLE NUMBER
Antimony
Arsenic
Barium
Beryllium
Cadmium
Calcium
Chromium
Cobalt
Copper
Iron
lead
Manganese
Mercury
Nickel
Selenium
Tellurium
Tin
Titanium
Vanadium
Zinc
Chloride
Fluoride
Nitrates
Sulfates
592*
—
-- •
_ - . .
. — "
— '
_ '
—
— "'.
—
—
— '
o.u
_ .
— •
—
• —
—
— *
— •
—
— •
--— .
757*
•.—
.
._
—
—
—
—
—
•
— '
—
i-
0.5
—
—
—
—
—
—
'
740*
' —
1-700
'_—
—
— '
—
— '
—
—
—
—
—
O.W
r- \
— '
— •
—
—
—
—
/30
OS
^6 & ^rOa9
^J^J ^) 1 i
0.33
/.IO
-------
13- Wood Bark Boiler
Test 13-18
TABLE Downstream of Precip.-coal 8 wood fi
el
POLLUTANT
SAMPLE NUMBER
Antimony
Arsenic
Barium
Beryllium
Cadmium
Calcium
Chromium
Cobalt
Copper
Iron
Lead
Manganese
Mercury
Nickel
Selenium
Tellurium
Tin
Titanium
Vanadium
Zinc
Chloride
Fluoride
Nitrates
Sulfates
0* dupl.
O.fe
-------
13- Wood Bark Boiler
Test 13-18 TABLE Downstream of Precip.-coal 6 wood fi
POLLUTANT SAMPLE NUMBER
Antimony
Arsenic
Barium
Beryllium
Cadmium
Calcium
Chromium
Cobalt
Copper
Iron .
Lead
Manganese
Mercury
Nickel
Selenium
Tellurium
Tin ,
Titanium
Vanadium
Zinc
Chloride
Fluoride >
Nitrates
[Sulfat«s
1032+
-------
COMMERCIAL TESTING & ENGINEERING CO.
OENEHAL OFFICE*: «»• NORTH LA IALLE *T*EET, CHICAOO, ILLINOIS *OeOI • A*EA CODE 119 79|.«4»4
Reply to iNSiiUMiNTAi ANAITSIS DIVISION. 1013 WEST «IH AVINUE. COIDIN. COIOIADO KHOI. PHONI, xa-vt-vat
To: Mr. John G. Michalovic
Calspan Corporation
Post Office Box 235
Buffalo, NY 14221
P. 0. No.: 27810 ^ p
Sample No.: 13 - 18 A 392 *
A
MM
")O *
""" Date: April 23, 1977
Analyst: S. Sweeney
IAD No.: 97-A197-134-31
CONCENTRATION IN PPM WEIGHT
ELEMENT CONC.
Uranium
-------
COMMERCIAL TESTING fit ENGINEERING CO.
SENEGAL orncES: »i NORTH LAIALLE *T*ecT, CHICAOO, ILUNOII eoioi • AREA CODE «ia 7je-MM
Reply to iNSinuMiNTAi ANALYSIS DIVISION, taas WEST «TH AVENUE. GOIDEN. COIOBADO KUOI. PHONE.
To: Mr. John G. Michalovic ^Sl^L
Calspan Corporation ^^51.5^^
Post Office Box 235
Buffalo, NY 14221
P. 0. No.: 27810
Sample No.: 13 - 18 B
737 "V *
>\
CONCENTRATION
ELEMENT
Uranium
thorium
Bismuth
Lead
Thallium
Mercury
Gold
Platinum
Iridium
Osmi urn
Rhenium
Tungsten
Tantalum
Hafnium
Lutetium
Ytterbium
Thulium
Erbium
Hoi mi urn
Dysprosium
CONC.
15
11
2
190
23
NR
<0.1
6
<0.7
1
0.5
2
0.3
1
3
4
ELEMENT
Terbium
Gadolinium
Europium
Samarium
Neodymium
Praseodymium
Cerium
Lanthanum
Barium
Cesium
Iodine
Tellurium
Antimony
Tin
Indium
Cadmi urn
Silver
Palladium
Rhodium
.-
CONC.
0.9
3
1
9 -
24
11
62
37
MC
7
10
<0.5
21
19
STD
3
11
2
IN PPM WEIGHT
ELEMENT
Ruthenium
Molybdenum
Niobium
Zirconium
Yttrium
Strontium
Rubidium
Bromine
Selenium
Arsenic
Germanium
Gallium
Zinc
Copper
Nickel
Cobalt
Iron
Manganese
Chromi urn
t
Date: April 23, 1977
Analyst:
IAD No.:
CONC.
95
24
230
70
MC
610
41
58
MC
MC
780
MC
960
290
32
MC
MC
810
S. Sweeney
97-A197-134-31
ELEMENT
Vanadium
Titanium
Scandium
Calcium
Potassium
Chlorine
Sulfur
Phosphorus
Silicon
Aluminum
Magnesium
Sodium
Fluorine
Oxygen
Ni trogen
Carbon
Boron
Beryl 1 i urn
Lithium
Hydrogen
CONC.
530
MC
41
MC
MC
400
MC
MC
MC
MC
MC
MC
=MC
NR
NR
NR
MC.
1
37
NR
NR - Not Reported
All elements not reported
-------
COMMERCIAL TESTING & ENGINEERING CO.
Reply to
ernoui tti NORTM t» §»tn titter, ONIOACO, IUINOII teiei • AM* cool in m-*4M
IMTMMUNTAl. ANAIYM MVIIION. I4HS WMI 44TM AVINUI. OOIMN. COIMADO KUOI. PMOMIi JW.JTWSJ1
To. Mr. John G. Mlchalovlc ^t
Calspan Corporation ^^£
Post Office Box 235
Buffalo. NY 14221
\
P.O. No.. 27810 ] JMl
SempleNo.. 13 - 18 C 740. 282 W T .
Date: April 23. 1977
Aiwlyit. s. Sweeney
r\
IADNo.,97-A197-134-31
CONCENTRATION IN PPM WEIGHT
ELEMENT
Uranium
Thorium
Bismuth
Lead
Thallium
Mercury
Gold
Platinum
IHdlum
Osmium
Rhenium '
Tungsten
Tantalum
Hafnium
Lutetlum
Ytterbium
Thulium
Erbium
Hoi ml urn
Dysprosium
CONC.
13
16
9
MC
48
NR
-------
COMMERCIAL TESTING & ENGINEERING CO.
BENEIAL OFFICE*: Ml NORTH LA tALLE 1THEET. CHICAOO, ILIIHOK »«0t • AREA CODE 119 T9I-I414
Reply to INSTIUWNTM ANALYSIS DIVISION, MIIS war urn Avenue. cotofN. COIOIADO KMOI, rMONt, JOJ-JTMSJI
To: Mr. John G. M1chalov1c
Calspan Corporation
Post Office Box 235
Buffalo, NY 14221
•P.O. No.: 27810
Sample No.: KVB 13_18 0 530
Date: April 22, 1977
Analytt: s. Sweeney
IAD No.: 97-A197-134-31
CONCENTRATION IN PPM WEIGHT
ELEMENT CONC.
Uranium
Thorium
Bismuth
Lead <0.9
Thallium
Mercury NR
Gold
Platinum
Iridium
Osmi urn
Rhenium
Tungsten
Tantalum
Hafnium
Lutetium
Ytterbium
Thulium
Erbium
Holmium
Dysprosium
ELEMENT CONC.
Terbium
Gadolinium
Europium
Samarium
Neodymium
Praseodymium
Cerium
. Lanthanum
Barium 0.8
Cesium
Iodine <0.2
Tel 1 uri urn
Antimony
Tin
Indium STD
Cadmium <0.4
Silver 0.7
Palladium
Rhodium
ELEMENT
Ruthenium
Molybdenum
Niobium
Zirconium
Yttrium
Strontium
Rubidium
Bromine
Selenium
Arsenic
Germanium
Gallium
Zinc
Copper
, Nickel
Cobalt
Iron
Manganese
Chromium
CONC.
3
2
0.2
4
<0.1
0.7
0.2
<0.2
3
3
'3
<0.1
9.
0.4
6
*
ELEMENT
Vanadium
Titanium
Scandium
Calcium
Potassium
Chlorine
Sulfur
Phosphorus
Silicon
Aluminum
Magnesium
Sodium
Fluorine
Oxygen
Ni trogen
Carbon
Boron
Beryllium
Lithium
Hydrogen
CONC.
<0.1
1
-------
COMMERCIAL TESTING & ENGINEERING CO.
GENERAL OrriCEt: «• NORTH LA tALLE STREET, CHICAGO, ILLINOIS 80601 • AREA OoOE »'» »J§-»414
Reply to iNSTHiMiNtAi ANALYSIS DIVISION, ttat WIST MTH AVENUE. GOIDEN. COIOBADO acuoi, rnoM,
T0: Mr. John G. Michalovic
Calspan Corporation
Post Office Box 235
Buffalo, NY 14221
P. O. No.: 27810
Sample No.: 13_18 E
Date: April 23, 1977
Analyst: S. Sweeney
264, 331, 346, 528, 516. 517, 518 IAD No': 97-A197-134-31
CONCENTRATION IN
ELEMENT
Uranium
Thorium
Bismuth
Lead
Thallium
Mercury
Gold
Platinum
Iridium
Osmi urn
Rhenium
Tungsten •
Tantalum
Hafnium
Lutetium
Ytterbium
Thulium
Erbium
Hoi mi urn
Dysprosium
CONC. ELEMENT CONC.
Terbium
Gadolinium
<0.008 Europium
0-03 samarium
Neodymi urn
NR Praseodymi urn
Cerium 0.005
Lanthanum 0.01
Barium 0.05
Cesium <0.002
Iodine
Tel 1 uri urn
"Antimony
Tin
Indium STD
Cadmium <0.007
Silver MC
Palladium
Rhodi urn
ELEMENT
Ruthenium
Molybdenum
Niobium
Zirconium
Yttrium
Strontium
Rubidium
Bromi ne
Selenium
Arsenic
Germanium
Gallium
Zinc
Copper
Nickel
Cobal t
Iron
Manganese
Chromium
CONC.
0.05
0.01
0.02
0.002
0.009
<0.01
<0.002
<0.004
0.08
0.2
0.6
0.02
2
0.06
1
ELEMENT
Vanadium
Titanium
Scandium
Calcium
Potassium
Chlorine
Sulfur
Phosphorus
Silicon
Aluminum
Magnesium
Sodium
Fluorine
Oxygen
Ni trogen
Carbon
Boron i
Beryllium
Lithium
Hydrogen
CONC.
0.003
0.05
<0.003
3
MC
0.3
MC
0.8
0.3
0.6
0.5
MC
=0.04 .
NR'
NR
NR
0.2
0.009
NR
NR - Not Reported
All elements not reported < 0.004
Sample was thermally ashed 0 350° C for one
prior to analysis.
.
Approved:
hour in a laboratory
iiijnace in a quartz crucible
745
-------
COMMERCIAL TESTING & ENGINEERING CO.
atNIIAL OPPIOCIi III NORTH lAlALlC II»11T, CHICAGO. UllNOIt 10(01 • A*IA CODl (It TII-I4I4
R«ply IO INITIUMIN1AI ANAlVllt DIVISION. 14113 WIST 441H AVINUI, OOIDIN. COIOIADO 10401. fHONIi JOW7MMI
T0! Mr. John M1chalov1c
Calspan Corporation
Post Office Box 235
Buffalo, NY 14221
21k
P.O. No.: 27810
Sample No., 13 -18 E 12 264, 331, 346, 528, 516. 517, 518
CONCENTRATION IN
Date: April 23, 1977
Analyst: S. Sweeney
i
IAD No.: 97-A197-134-31
ELEMENT CONC.
Uranium
Thorium
Bismuth <0.008
Lead 0.03
Thallium
Mercury NR
Gold
Platinum
Irldlum
Osmium
Rhenium
Tungsten
Tantalum
Hafnium
Lutetlum
Ytterbium
Thulium
Erbium
Hoi ml urn
Dysprosium
ELEMENT CONC.
Terbium
Gadolinium
Europium
Samarium
Neodymlum
Praseodymium
Cerium 0.005
Lanthanum 0.01
Barium 0.1
Cesium <0.003
Iodine 0.009
Tellurium
Antimony
Tin
Indium STD
Cadmium <0.007
Silver MC
Palladium
Rhodium
NR - Not Reported
All elements not reported <0. 004 pg/ml
Sample was thermally ashed 9 350° C for one
EiEMENT
Ruthenium
Molybdenum
Niobium
Zirconium
Yttrium
Strontium
Rubidium
Bromine
Selenium
Arsenic
Germanium
Gallium
Z1nc
Copper
Nickel
Cobalt
Iron
Manganese
Chromium
Approved: :
hour In a la
CONC.
0.1
0.02
0.009
0.003
0.009
<0.02
<0.004
<0.004
QS.l
0.06
0.3
0.02
2
0.09
1
/
boratopy
ELEMENT
Vanadium
Titanium
Scandium
Calcium
Potassium
Chlorine
Sulfur
Phosphorus
Silicon
Aluminum
Magnesium
Sodium
Fluorine
Oxygen
Nitrogen
Carbon
Boron
Beryllium
Lithium
Hydrogen
furnace 1n a
CONC.
0.008
0.02
<0.001
2
4
0.2
MC
0.5
0.7
0.2
0.05
4
=0.06
NR
NR .
NR
0.9
0.002
^
quartz crucibl
prior to analysis.
746
-------
" My to i
COMMERCIAL TESTING & ENGINEERING CO.
BENERAl OFFICES: 991 NORTH LA SAllt STREET. CHICAOO, ILUNOI1 tO>01 • AREA CODE »I3 79>-*4l4
INiHUMlNlAl ANAlTSli DIVISION. 14115 WEST 441H AVINUl. COlOiN. COIOIADO tOU>\. FHONl, M1-17I.V52I
To: Mr. John G. Michalovic
Calspan Corporation
Post Office Box 235
Buffalo, NY 14221
P. O. No.: 27810
Date: April 23, 1977
Analyst: S. Sweeney
Sample No.: /}~/y t /
ELEMENT CONC.
Uranium
Thorium
Bismuth ^. 0,00?
Lead 0. t> 3
Thallium
.•rcury fjf.
Gold
Platinum
Iridium
Osmium
Rhenium
Tungsten
Tantalum
Hafnium
Lutetium '
Ytterbium
Thul i urn
Erbium
Hoi mi urn
Dysprosium
NR - Not Reported
7't>. / j / IAD No.: 97-A197-134-31
CONCENTRATION IN PPM WEIGHT
ELEMENT CONC.
Terbi urn
Gadolinium
Europium
Samarium
Neodymi urn
Praseodymium
Cerium 0,0 of
Lanthanum 0. 0 1
Barium 0,07?
Cesium < o.vz- f
Iodine ff,folfff
Tellurium
Antimony
tin
Indium sro
Cadmium <. 0.00?
Silver fl c
Palladium
Rhodium
ELEMENT CONC.
Ruthenium
Molybdenum e.677
Niobium
Zirconium 0. e>tf
Yttrium
Strontium 0.oM5~
Rubidium 0, 003. 5~
Bromine 0.00^
Selenium <0. 0fS~
Arsenic < 0. 00 J
Germanium
Gallium < 0,001
Zinc O.01
Copper o. 1 3
Nickel 0. VS~
Cobalt 0- 03-
Iron 2.
Manganese 0.07?
Chromium /
x7/7>* U
ELEMENT CONC.
Vanadium 0.0o?f
Titanium ?>"
Scandium <.e* 002.
Calcium 2.^,
Potassium V < M C
Chlorine ^. 2. S~
Sulfur ''/t c
Phosphorus 0. fS~
Silicon 0. 5"
Aluminum *• V
Magnesium 0.2 75"
Sodium V < tfc
Fluorine 0.e>5~
Oxygen fJ&
•i
Nitrogen fJK.
Carbon V &.'
Boron 0.??
Beryllium .
Lithium e.e>ef5~
Hydrogen /^
n.^ ^^^
Aooroved:
747
-------
COMMERCIAL TESTING & ENGINEERING CO.
GENERAL OFFICES: 1» NOHTH LA IALLE 1THECT. CHICAGO, ILLINOIf (0(01 • A*EA CODE ill 79«->4l4
Reply tO i . INSTBUMEN1AL ANALYSIS DIVISION. 14115 WIST 44TH AVENUE. GOIDEN. COLORADO (0401. PHONE: J03-77».952I
To: Mr. John Michalovic
Calspan Corporation
Post Office Box 235
Buffalo, New Y6rk
14221
P.O. No.: 27810
Sample No.: KVB 13-18 G 420
Date: April 22. 1977
Analyst: s. Sweeney
IAD No.: 97-Al 97-134-31
CONCENTRATION IN PPM WEIGHT
ELEMENT CONC.
Uranium
. Thorium
Bismuth
Lead <2
Thallium
Mercury NR
Gold
Platinum
Iridium
Osmi urn
f
Rhenium
Tungsten
Tantalum
Hafnium
Lutetium
Ytterbium
Thulium
Erbium
Hoi mi urn
Dysprosium
ELEMENT CONC.
Terbium
Gadolinium
Europium
Samarium
Neodymi urn
Praseodymium
Cerium
Lanthanum
Barium . <1
Cesium
Iodine
Tellurium
Antimony
Tin
Indium STD
Cadmium <1
Silver £0.8
Palladium
Rhodi urn
. NR - Not Reported
. All elements not reported <0. Sppm weight
Sample was thermally ashed 9400° C for in
ELEMENT CONC.
Ruthenium
Molybdenum 3
Niobium
Zirconium 3
Yttrium
Strontium £0.3
Rubidium
Bromi ne
Selenium
Arsenic £0.3
Germanium
Gallium
Zinc 4
Copper 1
Nickel 0.7
Cobalt £0.1
Iron 2
Manganese 0.1
Chromium 3
/.
Approved: ff((/l/^'
a laboratory oven i/i a
ELEMENT
Vanadium
Titanium
Scandium
Calcium
Potassium
Chlorine
Sulfur
Phosphorus
Silicon'
Aluminum
Magnesium
Sodium
Fluorine '
Oxygen
Ni trogen
Carbon
Boron
Beryllium
Lithium
Hydrogen
CONC.
0.2
2
£0.004
30
29 .
2
4
13
40
2
20
30
*5
NR
NR
NR
4
0.2
NR
JTi
\^^-^J^
quartz crucible prior
anal we
748
-------
COMMERCIAL TESTING & ENGINEERING CO.
GENERAL OFFICES: Ml NORTH LA (AI.I.E (TREET. CMICAOO, ILLINOIS 10*01 • AREA CODE (It 7»«-»4»4
Reply to iNsmiMiNiAi ANALYSIS DIVISION. \tai wui MTH AVINUE. cotMN. COIOIADO RMOI. moNti jon7»*ai
To: Mr. John G. Michalovic jfclBik.
Calspan Corporation •— —
Post Office Box 235
Buffalo, New York
14221
P.O. No.: 27810
Sample No.: KVB 13-18 H
ELEMENT CONC.
Uranium <0.07
Thorium
Bismuth
Lead <0.04
Thallium
Mercury NR
Gold
Platinum
Iridium
Osmi urn
Rhenium
Tungsten
Tantalum
Hafnium
Lutetium
Ytterbium
Thulium
Erbium
Hoi mi urn
Dysprosium
339
CONCENTRATION
ELEMENT CONC.
Terbium
Gadolinium
Europi urn
Samarium
Neodymium
Praseodymi urn
Cerium
Lanthanum
Barium 0.02
Cesium
Iodine
Tellurium
Antimony
Tin
Indium STD
Cadmium <0.02
Silver MC
Palladium
Rhodi urn
NR - Not Reported
All elements not reported <0. 008 pQ/mT
SamnlP wa<; thermal! v ashed 0300° C for one
IN yg/ml
ELEMENT
Ruthenium
Molybdenum
Niobium
Zirconium
Yttrium
Strontium
Rubidium
Bromine
Selenium
Arsenic
Germanium
Gallium
Zinc
Copper
Nickel
Cobalt
Iron
Manganese
Chromi urn
f
Approved: /
hour in a la
Date: April 22. 1977
Analyst: s. Sweeney
IAD No.:
CONC.
0.05
, 0.05
0.02
0.02
<0.03
<0.004
0.06
0.05
0.1
<0.005
0.5
0.04
0.1
97-A1 97-1 34-31
ELEMENT
Vanadium
Titanium
Scandium
Calcium
Potassium
Chlorine
Sulfur
Phosphorus
Silicon
Aluminum
Magnesium
Sodium
Fluorine
Oxygen
N1 trogen
Carbon
Boron
Beryllium
Lithium
Hydrogen
!
CONC.
0.003
0.05
£0.002
4
6
0.5
MC
3
1
0.1
270
8
-0.2
NR
NR
NR
0.02
0.005
NR
w.%^^
Dora/triry/oven in a quartz crucibli
749
-------
COMMERCIAL TESTING & ENGINEERING CO.
eCNCDAL OFFICE*: »• NORTH LA SALLE STREET, CHICAOO, ILLINOIS sosoi • AREA CODE aia ra*-s4i4
Reply tO INSTIUMINTAl ANALYSIS DIVISION. I«U5 WtST MTH AVENUE. GOLDEN. COlOtADO KMOI. FHONE. JOJ.17S49I
To: Mr. John G. Michalovlc
Calspan Corporation
Post Office Box 235
Buffalo. NY 14221
P.O. No.: 27810
S.mple No.: Kvp, 13_18 j 1032
Date: April 22, 1977
$. Sweeney
IAD No.: 97-A197- 134-31
CONCENTRATION IN PPM WEIGHT
ELEMENT
Uranium
Thorium
Bismuth
Lead
Thallium
Mercury
Gold
Platinum
Irldlum
Osmium
Rhenium
Tungsten
Tantalum
Hafnium
Lutetlum
Ytterbium
Thulium
Erbium
Kolmlum
Dysprosium
CONC.
2
3
«>.3
60
0.7
NR
fp.8
<0.3
<1
0.4
0.6
ELEMENT
Terbium
Gadolinium
Europium
Samarium
Neodymium
Praseodymium
Cerium
Lanthanum
Barium
Cesium
Iodine
Tellurium
Antimony
Tin
Indium
Cadmium
Silver
Palladium
Rhodium
CONC.
0.2
0.5
0.3
2
4
0.9
10
7
MC
0.5
0.5
<0.5
0.9
12
STD
1
27
±2
ELEMENT
Ruthenium
Molybdenum
Niobium
Zirconium
Yttrium
Strontium
Rubidium
Bromine
Selenium
Arsenic
Germanium
Gallium
Z1nc
Copper
Nickel
Cobalt
Iron
Manganese
Chromium
CONC.
2
2
7
2
530
95
19
4
15
2
12
MC
550
23
6
.MC
MC
37
ELEMENT
Vanadium
Titanium
Scandium
Calcium
Potassium
Chlorine
Sulfur
Phosphorus
Silicon
Aluminum
Magnesium
Sodium
Fluorine
Oxygen
Nitrogen
Carbon
Boron
Beryllium
Lithium
Hydrogen
CONC.
10
430
2
MC
MC
MC
MC
MC
MC
>170
MC
>420
«110
NR
NR
NR
150
€0.1
0.9
NR,
NR - Not Reported
All elements not reported <0.2 ppm weight
Sample was thermally ashed for. one hour
375'
one
1/r a laboratory furnace In a
750
-------
R«ply to
COMMERCIAL TESTING & ENGINEERING CO.
•INHAI. OMioitt t>i NOITH LA t*iLt tTHttr, CHICAOO, IUINOII (0101 •' AM* oooi §ia tt*.i4i4
"• INinUMINIAl ANAlYSli DIVISION, I4JJJ WU1 44TM AVINUI. OOIMN, CWOtAOO (MO). FHONti MMTMfll
To: Mr. John G. M1chalov1c f\
Calspan Corporation ^H?
Post Office Box 235
Buffalo, HY 14221 :
P. 0. No., 27810 ^ \wk\*
Sample No., KVB 13-18 K 1033 ^O>
CONCENTRATION
ELEMENT
Uranium
Thorium
Bismuth
Lead
Thallium
Mercury
Gold
Platinum
Irldlum
Osmium
Rhenium
Tungsten
Tantalum
Hafnium
Lutetlum
Ytterbium
Thulium
Erbium
Hoi ml urn
Dysprosium
CONC.
11
27
<0.2
6
0.4
NR
0:8
3>.5
3
0.5
3
0.2
1
2
5
NR - Not Reported
All. elements not reported
ELEMENT
Terbium
Gadolinium
Europium
Samarium
Neodymlum
Praseodymium
Cerium
Lanthanum
Barium -
Cesium
Iodine
Tellurium
Antimony
Tin
Indium
Cadmium
Silver
Palladium
Rhodium
<0.2ppm weight
CONC.
0.6
4
2
13
39
16
160
97
-MC
17
0.1
0.4
1
STD
10. 2
0.1
75
"" Date, April 22, 1977
Analyst, S. Sweeney
IAD No., 97-A179-134-31
IN PPM WEIGHT
ELEMENT
Ruthenium
Molybdenum
Niobium
Zirconium
Yttrium
Strontium
Rubidium
Bromine
Selenium
Arsenic
Germanium
Gallium
Z1nc
Copper
Nickel
Cobalt
Iron
Manganese
Chromium
Approved: -'/J
'. • f
\
CONC.
2
32
360
46 ' '
560 '
480
5
4
2
3
37
37
38
39
11
MC
140
400
ELEMENT
Vanadium
Titanium
Scandium
Calcium
Potassium
Chlorine
Sulfur
Phosphorus
Silicon
Aluminum
Magnesium
Sodium
Fluorine
Oxygen
N1 trbgen
Carbon
Boron
Beryllium
Lithium
Hydrogen
^^A
CONC.
210
MC
33
MC'
MC
18
>870
.MC
MC
MC
MC
MC •
•110
NR
NR
NR
29
0.5
>390
NR
-------
COMMERCIAL TESTING & ENGINEERING CO.
QtNCDAl OmCtS: »> NOHTH LA 1ALIE tTREET. CHICAQO, IIUNOII (0101 • AHEA CODE 119 79«-(414
Reply to iNSiiuMiNtM ANALYSIS DIVISION. 14111 wisi MTH AVINUI. COIOIN. COUWADO toot. PHONE. xant-9a\
TO: Mr. John Michaloyic
Calspan Corporation
Post Office Box 235
Buffalo, New York
14221
P.O. No.= 27810
Sample No.: KVB 13-18L 1034
Date: /\prn 22, 1977
Anal/**.- 5. Sweeney
IAD No.: 97-Al 97-134-31
CONCENTRATION IN PPM WEIGHT
ELEMENT
Uranium
Thori urn
Bismuth
Lead
Thallium
Mercury
Gold
Platinum
Iridium
Osmium
Rhenium
Tungsten
Tantalum
'Hafnium
Lutetium
Ytterbium
Thul i urn
Erbium
Hoi mi urn
Dysprosium
CONC. .
14
17
0.2
58'
7
NR
x
<0.1
2
<0.8
2
0.5
2
0.2
2
3
4
ELEMENT
Terbium
Gadolinium
Europium
Samarium
Neodymi urn
Praseodymi urn
Cerium
Lanthanum .
Barium
Cesium
Iodine
CONC.
0.9
2
1
9
21
7
56
40
MC
6
1
Tellurium
-------
Test No.
TRACE SPECIES AND ORGANICS TEST
SAMPLE RECOVERY LOG
Date //-//- 76 Location /3-
Saniple Port Position
Vic SeiAS EXCEPT
%•
Uo
TtB
Container
Number
73*
73 /
73 5*
tot
19*
to)
-fer
-TO*
Sample Description
ao*/t>s.
s •*/ f/i rsx.
3 x^ iJ/93/f
-l Ct>*>l>CS3/9T£
^- itnPjtle.**.
&.**>*.
/<*»/
Container
Type
^*
fj
/Jl AHu.ee*>
//
AiVL&t'J
*>t *.&£*>
93
1
3V.
Data Sheet KVB 6002-15
753
-------
TRACE SPECIES AND ORGANICS TEST
SAMPLE RECOVERY LOG
Test No. 13-34 Date
Sample Port Position
Location <2> - L3oct3-l*>AJtX
OP T:faBg-V^>. CTe^A.1. ^- idoo'b,
IS-24I
Container
Number
1055
103k
i car?
B
Sample Description
Sst:
-5
-2.
IS kd*. MM & -t-£l&
- 2.4
L"B
VB
UB,
Container
Type
Net
wt/vol.
Vls-T
Tfeo Ji
Comment
SbSSaz.
Data Sheet KVB 6002-15
754
-------
13- Wood Bark Boiler
Test 13-24 TABLE Downstream of Precip.-coal & wood fi
POLLUTANT SAMPLE NUMBER
Antimony
Arsenic
Barium
Beryllium
Cadmium
Calcium
Chromium
Cobalt
Copper
Iron
Lead
Manganese
Mercury
Nickel
Selenium
Tellurium
Tin
Titanium
Vanadium
Zinc
Chloride
Fluoride
Nitrates
Sulfates
739+
<»*rfo
/vo
^•2,0
1
l(~
/OOODO
7«/0
<~70
/feo
•33000
3-10
•3900
7.4
no
1-7
•000
Vfeoo
720
7300
—
~ i
731+
o
-------
13 - Wood Bark Boiler
Test 13-24 TABLE Downstream of. Precip. -coal & wood f
POLLUTANT SAMPLE NUMBER
Antimony
Arsenic
Barium
Beryllium
Cadmium
Calcium
Chromium
Cobalt
Copper
Iron
Lead
Manganese
Mercury
Nickel
Selenium
Tellurium
Tin
Titanium
Vanadium
Zinc
Chloride
Fluoride
Nitrates
V
V}
\
0
>
—
-—
o.VS
Sulfates l"7^0O
503*
^o.S
*l
-------
13-Wood Bark Boiler
Test 13-24' TABLE Downstream of Precip.-coal & wood f\
POLLUTANT SAMPLE NUMBER
Antimony
Arsenic
Barium
Beryllium
Cadmium
Calcium
Chromium
Cobalt
Copper
Iron
Lead
Manganese
Mercury
Nickel
Selenium
Tellurium
Tin
Titanium
Vanadium
Zinc
Chloride
Fluoride
Nitrates
1037+
bO
33000
/"io
130
-------
COMMERCIAL TESTING & ENGINEERING CO.
Reply to INSTRUMENTAL
ANALYSIS DIVISION, 14135 WESI 44TH
AVENUE, GOLDEN. COLORADO 60401. PHONE: 303 3769531
To; Mr. John G. Michalovic • jfltSL.
Calspan Corporation •—••«
Post Office Box 235
Buffalo, New York
14221
P.O. No.: 27810 A
Sample No.: KVB 13-24 #503
Date: April 22, 1977
Analyst: 5. Sweeney
IAD No.: 97 -Al 97-1 34-31
CONCENTRATION IN Jig/ml
ELEMENT CONC.
Uranium ID-OS
Thorium
Bismuth
Lead IP.04
Thallium
Mercury NR
Gold
Platinum
Iridium
Osmium
Rhenium
Tungsten
Tantalum
Hafnium
Lutetium
Ytterbium
Thulium
Erbium
Hoi mi urn
Dysprosium
ELEMENT CONC.
Terbium
Gadolinium
Europium
Samarium
Neodymi urn
Praseodymium
Cerium
Lanthanum
Barium . 0.02
Cesium
Iodine
Tellurium
Antimony
Tin
Indium STD
Cadmium ±0.01
Silver
Palladium
Rhodium
ELEMENT
Ruthenium
Molybdenum
Niobium
Zirconium
YUri urn
Strontium
Rubidium
Bromine
Selenium
Arsenic
Germanium
Gallium
Z1nc
Copper
Nickel
Cobalt
Iron
Manganese
Chromium
CONC.
0.1
0.1
0.007
<0.03
<0.004
0.03
0.05
0.01
<0.003
*0.1
0.002
0.005
ELEMENT
Vanadium
Titanium
Scandium
Calcium
Potassium
Chlorine
Sulfur
Phosphorus
Silicon
Aluminum
Magnesium
Sodium
Fluorine
Oxygen
Nitrogen
Carbon
Boron
Beryllium
Lithium
Hydrogen
CONC/
0.003
0.05
<0.001
1
*0.4
0.3
0.2
0.3
*1
' *0.06
0.02
0.3
']
NR
NR
NR
0.02
0.001
NR
NR - Not Reported
All elements not reported <0. 008
Approved:
^Heterogeneous - Sample was thermally ashed 0350° C for
ven
758
-------
ly to
COMMERCIAL TESTING & ENGINEERING CO.
acNeiiAi orncit. in NORTH LA IAUC ITHCIT, CHICAOO, U.LINOK toioi • ACCA coot lit *n-t4»4
INSTIUMINIAl ANAITIII DIVItlON, IUJJ Will 441N AVINUl. OOIDIN, COIOIADO 10401. FHONIi MU.J7»-9J3I
''•"• Mr. John G. M1chalov1c .^Cl^^.
Calspan Corporation ^^SrJ^^
Post Office Box 235
Buffalo, NY 14221" " —
P. O. No.: 27810 £
Sample No.-. KVB 13-24 506
Date: April 22, 1977
Analyst: S. Sweeney
IAD No.-. 97-A197- 134-31
CONCENTRATION IN yQ/ml
ELEMENT CONC.
Uranium
Thorium
Bismuth
Lead fO.03
Thallium
Mercury MR
Gold
Platinum
Irldlum
Osmium
Rhenium
Tungsten
Tantalum
Hafnium
Lutetium
Ytterbium
Thulium
Erbium
Hoi ml urn
Dysprosium
NR - Not Reported
All elementl not reported
Sample was thermally
ELEMENT CONC.
Terbium
Gadolinium
Europium
Samarium
Neodymi urn
Praseodymium
Cerium
Lanthanum
Barium 0.03
Cesium
Iodine rato(>j/l
ELEMENT
Vanadium
Tttanlum
Scandium
Calcium
Potassium
Chlorine
Sulfur
Phosphorus
Silicon
Aluminum
Magnesium
Sodium
Fluorine
Oxygen
Nitrogen
Carbon
Boron
Beryllium
Lithium
Hydrogen
/ /
fe^^t
Furnace. 1'n a
CONC.
0.002
0.03
<0.001
1
0.6
0.3
0.1
0.6
0.6
0.008
0.5
0.2
-0.1
NR
NR
NR
0.02
0.005
NR
1
/
quartz crucible
orlor to analvjls.
759
-------
COMMERCIAL TESTING & ENGINEERING CO.
GENERAI. OFFICES: >•• NORTH I* SAILE »TKECT, CHICAGO. IIUNOII «0«01 • A*EA CODE *I9 TM-1414
Reply to iMTnuMiNiAi ANALYSIS DIVISION, tost WEST *ITM AVINUE. COIDEN. COIOIADO §o
-------
Mr. S. C. Hunter
-3-
KVB ANALYSIS DATA
SAMPLE
14 616
POM's
27 ug/1
PCB's
12/2 - 3 B
12/2 - 6 E
13/18 M
13/18 M deep
13/18 N
13/24 609
13/24 A
< 10 ug/1
10 ug/1
2480 ug/1
2890 ug/1
225 ug/1
234 ug/1
10 ug/1
< 1 ug/1
'1 ug/1
< 10 ug/1
<• 10 ug/1
-------
KVB Analysis Data
. ' •
Sample Number POM's . PCB's
298 < 1 ug/g < 1 ug/g
534 < 1 ug/g < 1 ug/g
534 (duplicate) < 1 ug/g < 1 ug/g
13V18 740 90 ug/g < 1 ug/g
13-18 282 ' 49 ug/g < 1 ug/g
13-18 -530 3.2 ug/g . < 1 ug/g
13-18 1038 6.3 ug/g < 1 ug/g
13-18 1032 396 ug/g < 1 ug/g
13-18 1033 1 ug/g < 1 ug/g
13-18 1034 8 ug/g < 1 ug/g
13-18 1034 (duplicate) 9 ug/g < 1 ug/g
13-24 735 513 ug/g < 1 ug/g
531 6.9 ug/g < 1 ug/g
1039 20 ug/g < 1 ug/g
1035 144 ug/g < 1 ug/g
1036 10 ug/g < 1 ug/g
1037 7.1 ug/g < 1 ug/g
1037 (duplicate) 8.5 ug/g < 1 ug/g
14 556 70.5 ug/g < 1 ug/g
568 .104 ug/g < 1 ug/g
532 10.7 ug/g < 1 ug/g
532 (duplicate)- 8.2 ug/g . < 1 ug/g
15-10 1041 < 0.1 ug/g < 1 ug/g
1041 (duplicate) < 0.1 ug/g < 1 ug/g
1042 * .-.':,*•
15-11 941 < lug/1 < lug/1
1044 <0.1 ug/g <1 ug/g
1045 * .•••••-
19-1 LF . * *
19-2 533 < 0.1 ug/g < 1 ug/g
533 (duplicate) < 0.1 ug/g <1 ug/g
C . <1 ug/1 <1 ug/1
C (duplicate) < 1 ug/1 < 1 ug/1
: LF .•*... *
*Sample extracts too concentrated to be able to determine an analytical valuej
762
-------
OPEN HEARTH FURNACE
Location No. 14" ! Unit No.
Unit Description
Installation Date 12>5"2-
Heater Rating 5~1 W\ ^ C \S>^> K^°"^:u^/ Lr )
CL 1 /-"
Burner Description O tpor r,ti.r f. ~~ *O i r
Too-r a^iJl \ a, T i? ?» c. L e. ^ ':4 .
\v4u*v>^3>.
Test Fuel Combinations ^s^A^T. C\kfi /\»J
'
^ Mo & 0,L Ci.34-XSuLf^N
j *
Fuel Temp, at Burner (°F) "- fp&o r:' /' Jor .1/$. /£ &.•'/
Primary Air Temp. (°F) 1 ^l.l K ( l^^^^F7 )
Comments:
763
-------
Test No.
Unit No.
MOBILE LABORATORY DATA
Date II' /7~7S Location
Test No.
Fuel
Capacity
Unit Type
Burner Type_
1. Test No.
2. Date
3 . Time
4. Load
5. Process Rate
6. Flue Diam. or Size, ft
7. Probe Position
8. Oxygen (%)
9. NOx (hot) read/3% 02 (ppm)
10. NO (hot) read/3% 02 (ppm)
11. NO? (hot) read/3% 02 (ppm)
12. NO (cold) read/3% O2 (ppm)
13. Carbon Dioxide (%)
14. Carbon Monoxide (ppm) uncor/cor
15. Hydrocarbon (ppm) uncor/cor
16. Sulfur Dioxide (ppm) uncor/cor
17. Smoke Spot (Bacharach)
0tY gvt-f s~\
18. Atmes"; — Temp; O?7 C)
19. Dew Point Temp. (°F/°C)
20. Atmos. Pressure (in. Hg)
21. Relative Humidity (%)
22.
23.
24.
25.'
26.
27.
28.
29.
30.
/i-i
n -17-76
13&0
l'-6"
&£UT£.«.
H.
720
*?W
2 &
2&o
/t>
to
20
I'll •
r
3Ftg
yftZ
5*6
2215
3- %
2g
5?
?l
?
&f
• M 1 ""•
X/
20
20
2^
/$&
f yft ^
0
t S jj JP
?Y
63
63
—
^Z
*/f
30>*1
S3
•
XT'-/
tt-f?~rf
/'/?&
cf#r£*
W,
_~
?00
?2?
-„
//
/o
W
5~
—
IZ&
• —
H5i
W
2?
ni
—
—
30.2-ff
—
/*/- 1
ii-ir-rf
/J-00
cgMrf*.
//'0
— ^~
—
~- —
ro 10
—
>209oi&(M
? *f
I620 23U
^_-
5~*2
V5~
?
-------
Test No. 11" f
Unit No.
MOBILE LABORATORY DATA
Date //~/7~~ So. Location
Fuel 0fl /&/4S Capacity
Test No.
Engr
Unit Type
Burner Type_
1. Test No.
2. Date
3. Time
4. Load
5. Process Rate
6. Flue Diam. or Size, ft
7. Probe Position
8. Oxygen (%)
9. NOx (hot) read/3% 02 (ppm)
10. NO (hot) read/3% 02 (ppm)
11. NO? (hot) read/3% 02 (ppm)
12. NO (cold) read/3% O2 (ppm)
Is. Carbon Dioxide (%)
14. Carbon Monoxide (ppm) uncor/cor
15. Hydrocarbon (ppm) uncor/cor
16. Sulfur Dioxide (ppm) uncor/cor
17. Smoke Spot (Bacharach)
Qff 1^" & ft 1 ff
18. Atmoai Tempr {^"C)
19. Dew Point Temp. ^F)f<'C)
20. Atmos. Pressure (in. Hg)
21. Relative Humidity (%)
22.
23.
24.
25.
26.
27.
28.
//'/
/l'/7-7{
/?.?H
$
30
—- - —
?r
23o
-------
Test No. '' I
Unit No.
MOBILE LABORATORY DATA
Date X/-/7-/V Location
Fuel 0fL/£4$ Capacity
Test No.
Engr.
Unit Type
Burner Type_
1. Test No.
2. Date
3. Time
4. Load
5. Process Rate
6. Flue Diam. or Size, ft
7. Probe Position
8. Oxygen (%)
9. NOx (hot) read/3% 0? (ppm)
10. NO (hot) read/3% 02 (ppm)
11. NO? (hot) read/3% 02 (ppm)
12. NO (cold) read/3% 02 (ppm)
13. Carbon Dioxide (%)
14. Carbon Monoxide (ppm) uncor/cor
15. Hydrocarbon (ppm) uncor/cor
16. Sulfur Dioxide (ppm) uncor/cor
17. Smoke Spot (Bacharach)
19. Dew Point Temp. (ffX'C)
20. Atmos. Pressure (in. Hg)
21. Relative Humidity (%)
22.
23.
24.
25.
26.
27.
28.
29.
30.
11-1
l}'t7~?S
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120
3.00
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5~2-
1 ^
70.2.*!
$~$
/I- 1
//-J7-7f
/%3&
. O
'100. WO
% /
-------
Test No.
Unit No.
Date
MOBILE LABORATORY DATA
Location
Test No.
Engr.
Fuel
Capacity_
Unit Type
Burner Type_
1. Test No.
2. Date
3. Time
4. Load
5. Process Rate
6. Flue Diam. or Size, ft
7. Probe Position
8. Oxygen (%)
9. NOx (hot) read/3% 02 (ppm)
10. NO (hot) read/3% 02 (ppm)
11. NO? (hot) read/3% 02 (ppm)
12. NO (cold) read/3% 02 (ppm)
13. Carbon Dioxide (%)
14. Carbon Monoxide (ppm) uncor/cor
15. Hydrocarbon (ppm) uncor/cor
16. Sulfur Dioxide (ppm) uncor/cor
17. Smoke Spot (Bacharach)
-ty? $£*•£ /*sv«-.
19. Dew Point Temp. H??)0C)
20. Atznos. Pressure (in. Hg)
21. Relative Humidity (%)
22.
23.
24.
25.
26.
27.
28.
29.
30.
/Y~
//-/*
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.—
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—
767
Data Sheet 6002-2
-------
Test No.
Unit No.
MOBILE LABORATORY DATA
Date //" /
/
—
—
—
/w
3-0
13
2-f
^Z
tf 6
30. W
3-?
^
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2-
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30./1
J7
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/S£f~
^^ 7&~fi<-
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/
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-------
Test No.
Unit No.
Date,
Fuel
MOBILE LABORATORY DATA
Location
Test No.
Engr.
Capacity_
Unit Type OfefJ ffMP.Tff fU,WtC£ Burner Type
1. Test No.
2. Date
3. Time
4. Load
5. Process Rate
6. Flue Diam. or Size, ft
7. Probe Position
8. Oxygen (%)
9. NOx (hot) read/ 3% ©2 (ppm)-
10. NO (hot) read/3% 02 (ppm)
11. NO? (hot) read/3% 02 (ppm)
12: NO (cold) read/3% 02 (ppm)
13. Carbon Dioxide (%)
14. Carbon Monoxide (ppm) uncor/cor
15. Hydrocarbon (ppm) uncor/cor
16. Sulfur Dioxide (ppm) uncor/cor
17. Smoke Spot (Bacharach)
PR V PVI & /-^
18. Atmos-.- Temp. (c£/°C)
19. Dew Point Temp. (SE?°C)
20. Atxnos. Pressure (in. Hg)
21. Relative Humidity^ (%)
22.
23.
24.
25.
26.
27.
28.
29.
30.
11-3
>2-2}-7£
/2 $£>
'e£A*7f£
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I57f
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/fee
Cf/UTf*
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-------
Test No. ll/~ 3
Unit No.
MOBILE LABORATORY DATA
Date H~2 ? -?£ Location
Test No.
Engr.
Capacity
Unit Type 0/£fiJ tf£/ftr#
Burner Type_
1. Test No.
2. Date
3. Time
4. Load
5. Process: Rate
6. Flue Diam. or Size, ft
7. Probe Position
8. Oxygen (%)
9. NOx (hot) read/3% 02 (ppm)
10. NO (hot) read/3% 02 (ppm)
11. NO? (hot) read/3% 02 (ppm)
12. NO (cold) read/3% 02 (ppm)
13. Carbon Dioxide (%)
14. Carbon Monoxide (ppm) uncor/cor
15. Hydrocarbon Jppm) uncor/cor
16. Sulfur Dioxide (ppm) uncor/cor
17. Smoke Spot (Bacharach)
PA Y &vt& ^-^
Ifl A tries . TOIPP. CF_r°C)
19. Dew Point Temp. (^F^'C)
20. Atmos. Pressure (in. Hg)
21. Relative Humidity (%)
22.
23.
24.
25.
26.
27.
28.
29. .
30.
/y~f
/}~2S-?f
}r*0
C/At7£fi.
M-
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17?
— —
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1127
t/2?
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30. 7 /
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v...
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i
770
Data Sheet 6002-2
-------
Test No._
Unit No.
Date
MOBILE LABORATORY DATA
Location ' /
Test No.
Engr.
Fuel X/6 + A)* 6 Capacity
Unit Type 0f£fiJ
Burner Type
1.. Test No. '.......
2. Date
3. Time
4. Load
5. Process Rate
6. Flue Diam. or Size, ft
7. Probe Position
8. Oxygen (%)
9. NOx (hot) read/ 3% 02 (ppm)
10. NO (hot) read/3% 02 (ppm)
11. NO? (hot) read/3% 02 (ppm)
12. NO (cold) read/3% 02 (ppm)
13. Carbon Dioxide (%)
14. Carbon Monoxide (ppm) uncor/cor
15. Hydrocarbon (ppm) uncor/cor
16. Sulfur Dioxide (ppm) uncor/cor
17. Smoke Spot (Bacharach)
18. Atmos. Temp. (°F/°C)
19. Dew Point Temp. (eF/°C)
20. Atmos. Pressure (in. Hg)
21. Relative Humidity (%)
22.
23. XMir crctff, juo fiJ?0
/7,
11/3
}02S
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ft3
2~
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5TO Iff
&2 W£
V'l
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—
7?
$~6
21.3-/
35* '
771
Data Sheet 6002-2
-------
Test,No._
Unit No.
Date
MOBILE LABORATORY DATA
Location
Test No.
Engr
Capacity_
Unit Type
Burner Type
1. Test No.
2. Date .'...'.
3. Time
4. Load
5. Process .Rate
6. Flue Diam. or Size, ft
7. Probe Position
8. Oxygen (%)
9; NOxJhot) read/3% 03 (ppm)
10. NO (hot) read/3% 02 (ppm)
ll. NO? (hot) read/3% 02 (ppm)
12. NO (cold) read/3% 02 (ppm)
13. Carbon Dioxide (%)
14. Carbon, Monoxide (ppm) uncor/cor
15. Hydrocarbon (ppm) uncor/cor
16. Sulfur Dioxide (ppm) uncor/cor
17. Smoke Spot (Bacharach)
18. Atnos. Temp. < (°F/°C)
19. Dew Point Temp. (^F/'C)
20. Atmos. Pressure (in. Hg)
21. Relative Humidity (%)
22.
23.
24.
25- '
26.
27.
28.
29". '"•••. ''.''. __j
3d.
&*&/*!£.
3-21-77
I2?0
cs/vr£/t
W.
£7$r
400
7?
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1,2,0
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25~
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7
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72
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2l-5~£
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}i?r?i(7
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2-f 73
32f £721
?
-------
Test No..
Quit No.
Date
MOBILE LABORATORY DATA
Location / /
Test No.
Engr. /?', &'.
Capacity
Quit Type
Burner Type_
1. Test No.
2. Date
3. Time
4. Load
5. Process Rate
6. Flue Diam. or Size, ft
7. Probe Position
8. Oxygen (%)
9. NOx (hot) read/ 3% 02 (ppm)
10. NO (hot) read/3% 02 (ppm)
11. NO? (hot) read/3% 02 (ppm)
12. NO (cold) read/3% 02 (ppm)
13. Carbon Dioxide (%)
14. Carbon Monoxide (ppm) uncor/cor
15. Hydrocarbon (ppm) uncor/cor
16. Sulfur Dioxide (ppm) uncor/cor
17. Smoke Spot (Bacharach)
18. Atroos. Temp. (°F/°C)
19. Dew Point Temp. (°F/°C)
20. Atmos. Pressure (in. Hg)
21. Relative Humidity (%)
22.
23.
24.
25.
26.
27.
28.
p9.
po.
n&w£
3-21-77
I5~t>0
Cf*JT£/Z.
3.0.
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—
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—
O
d
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—
4
70
5Tf
21.5$
V2
15 '30
-
J£,Z
g&
200
5~0
7^0
3 * *-*
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: 0
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322\
3032
/ft
2.6*3
^^*>
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/?
0
—
—
—
-
'
/S
750 1250
723" H7f
J.5 75-
750 235V
-------
Test No._
Unit No.
Date
MOBILE LABORATORY DATA
Location- If
TestJIcu
Fue 1 NG J- *6 JA
—
—
......
—
!
f
I
I
I '' t
•
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.
•
.'• "
...
<
j
774
Data Sheet 6002-2
-------
.Test No..
Unit No.
MOBILE LABORATORY DATA
Date 1-30-7 ? Location
Test No.
Engr.
capacity
Unit Type
Burner Type
1. Test No.
2. Date
3. Time
4. Load
5. Process Rate
6. Flue Diam. or Size, ft
7. Probe Position
8. Oxygen (%)
9. NOx (hot) read/ 3% 02 (ppm)
10. NO (hot) read/3% 02 (ppm)
11. N09 (hot) read/3% 02 (ppm)
12. NO (cold) read/3% 02 (ppm)
13. Carbon Dioxide (%)
14. Carbon Monoxide (ppm) uncor/cor
15. Hydrocarbon (ppm) uncor/cor
16. Sulfur Dioxide (ppm) uncor/cor
17. Smoke Spot (Bacharach)
18. Atmos. Temp. (°F/°C)
19. Dew Point Temp. (°F/eC)
20. Atmos. Pressure (in. Hg)
21. Relative Humidity (%)
22.
23.
24.
25.,
26.
27.
28.
29.
30.
ttt/ 0*
3'? 0*77
0
c£Hre*
IF.i
f V &
£J J f*
13
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4.
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l&f
tt^
1112
{
2.6
—
u
A/A
S0
$~3
W.f~8 •
£3
01?
-------
Test No._
Unit No.
MOBILE LABORATORY DATA
Date ?-?*-77 Location /*/
Test No.
Engr
Fuel //£ "*•//-£ Capacity_
Unit Type
Burner Type
1. Test No.
2. Date
3. Time
4. Load
5. Process Rate
6. Flue Diam. or Size, ft
7. Probe Position
8. Oxygen (%)
9. NOx (hot) read/3% 03 (ppm)
10. NO (hot) read/3% 02 (ppm)
11. NO^ (hot) read/3% ©2 (ppm)
12. NO (cold) read/3% 02 (ppm)
13. Carbon Dioxide (%)
14. Carbon Monoxide (ppm) uncor/cor
15. Hydrocarbon (ppm) uncor/cor
16. Sulfur Dioxide (ppm) uncor/cor
17. Smoke Spot (Bacharach)
18. Atmos. Temp. (°F/°C)
19. Dew Point Temp. (°F/°C)
20. Atmos. Pressure (in. Hg)
21. Relative Humidity (%)
22.
23.
24.
25.
26.
27.
28.
29.
30.
lt>* #2.
3-?0'77
1/30
cftirzt-
1 /
3 &o
250
&
Z50
2.
1
— •
to
^
7
l&*
utf
2.2?
112?
£
12
....
1?
4
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—
—
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1200
1?, /
tf75~
^Ifyo
25-
37^
f-
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—
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7 5
itel
Ifi3
U
12 U
t
2-f
-
31
£7
5~£
2*?,5'i
JT7
/230
/£
MS
5~2S
3$
313
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6
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20
0
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1575
I /C./
'33 7
/
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to
• —
—
—
—
776
Data Sheet 6002-2
-------
Test No._
Unit No.
MOBILE LABORATORY DATA
a'
Date 3"2^-77 Location tj
Test No.
Engr.
Fuel/t/£
Capacity
Unit Type
Burner Type_
1. Test No.
2. Date
3. Time
4. Load
5. Process Rate
6. Flue Diam. or Size, ft
7. Probe Position
8. Oxygen (%)
9. NOx (hot) read/3% Q2 (ppm)
10. NO (hot) read/3% 02 (ppm)
11. NO^ (hot) read/3%. Q2 (ppm)
12. NO (cold) read/3% 02 (ppm)
13. Carbon Dioxide (%)
14. Carbon Monoxide (ppm) uncor/cor
15. Hydrocarbon (ppm) ! uncor/cor
16. Sulfur Dioxide (ppm) uncor/cor
17. Smoke Spot (Bacharach)
18. Atnos. Temp. (°F/°C)
19. Dew Point Temp. (°F/°C)
20. Atmos. Pressure (in. Hg)
21. Relative Humidity (%)
22.
23.
24. , • . ' .
25.
26.
27.
28.
29.
30.
LOW
* - ?£.
y 2*
l
'
10
C?
6i3
3-/
—
&
^
j^
•>»
«*^
'6t>o •
•-.
^>*
— ._
*~>-
^jr
111
Data Sheet 6002-2
-------
OPERATING DATA
Location 14
Open Hearth
Test No.
W-t
Date
NOV.f 7.1176
I7./174
Tine
Can Flow (cfh x 1000)
71.0
71.
Furn. Press. , in. H.O
Air Flow, (c£a) x 10
Oxygen Flow, (cfh) x 10
32
7S
23
Oxygen Flow integr.
936 r.
Atom. Steam Flow, Ib/hr
12.
13.
Atom. Steam integr.
If 31*
Atom. Steam, Ib/gal setpoint
f't
Gat Flow. % of total Btu
fff
fe
Total Btu/hr x 10
13 €
13 1
t'i
Oil Flow, QPH
J2-0
330
Total Btu integr.
17ft* 0
17 fa.
I7f*
Checker Temp., *F
KSe> -1000
> 7(0 -2.000
Bath Temp. , °F
Oil Press .j p«ig
to
re
Oil Flow integr.
0: at North Bridaewall
CO at North Bridgewall
Time of Meaaurementa at
North Bridgewall
Coinmentsi t/-/7~7S
(for
-------
OPERATING DATA
Location 14
Open Hearth
Test No.
H-l
tt-l
Date
H-17-7*
//-f7'77
Time
Gas Flow (cfh x 1000)
75-
try
Furn. Press., in. H_0
Air Flow, (cfm) x 10
23-2S-.S-
23 -
2-t -
Oxygen Flow, (cfh) x 10
#2-
Oxygen Flow integr.
, f
fit* -2.
Atom. Steam Flow, Ib/hr
Atom. Steam integr.
. 7
?
3 ft '2 -3
Atom. Steam, Ib/gal setpoint
£.0
sr-i
Gas Flow. % of total Btu
So
Total Btu/hr x 10
Oil Flow, GPH
32.0
JfO
foe
33-*
Total Btu integr.
tm.
. 6
Checker Temp., "F
I7f£> -
Bath Temp., "F
J.32. f Sit: i
Oil Press., psig
67
10
70
Oil Flow integr.
Q: at North Bridgewall
CO at North Bridgewall
Time of Measurements at
North Bridgewall
Commentsi
forrOH
779
-------
OPERATING DATA
Location 14
Open Hearth
Test No.
Date
Tine
Gas Flow (cfh x 1000)
Furn. Press., in. H.O
Air Flow, (cfm) x 103
Oxygen Flow, (cfh) x 10
Oxygen Flow integr.
Atom. Steam Flow, Ib/hr
Atom. Steam integr.
Atom. Steam. Ib/gal setpoint
Gas Flow, % of total Btu
Total Btu/hr x 106
Oil Flow, GPH
Total Btu integr.
'Checker Temp., °F
Bath Temp. , eF
Oil Preoa., psig
Oil Flow integr.
0* at North Bridgewall
CO at North Bridgewall
Time of Measurements at
North Bridgewall
W'l
f/-/7'77
rf'.ee
0
*-,<
0
0
9? to. 2.
—
}?V2-.3
f.*/
ta
6
o
/7i1
t (2.0 -f 7&
—
—
3(5'1*S'
' \
/t-l
/t->7'77
/f'3 7 -7 7
/f:0£>
f~?
*-/.£>?-
zr-z*
36
8320,
-------
OPERATING DATA
Location 14
Open Hearth
Test No.
W-2.
Date
Tine
Gas Flow (cfh x 1000)
5-3
Furn. Press., in. H_0
Air Flow, (cfm) x 10J
'2-2.
Oxygen Flow, (cfh) x 10
33
Oxygen Flow integr.
8139.0
Atom. Steam Flow, Ib/hr
Atom. Steam integr.
. 3
. 3
Atom. Steam, Ib/gal setpoint
3-3
Gas Flow. % of total Btu
fe>
£0
Total Btu/hr x 10
/ft
Oil Flow, GPH
3/5"
Total Btu integr.
tt13.
in?.*
Checker Temp., °F
/f 20 '
Bath Temp. . °F
Oil Press., psig
75-
Oil Flow integr.
2 7(70*
V/\ N.
rV
. i
Marti!
iUy
aH
*
KJ
k
Comnentst
'I
78 1
-------
OPERATING DATA
Location 14
Open Hearth
Test No.
/•f'2-
Date
Time
is"-/?
//:
Gas Flow (cfh x 1000)
#6
Furn. Press., in. H.O
hi
Air Flow, (cfm) x 10
2-7-21
Oxygen Flow, (cfh) x 10
22
Oxygen Flow integr.
. 7
Atom. Steam Flow, Ib/hr
Atom. Steam integr.
Atom. Steam, Ib/gal setpoint
f,*
7.4
ft!
Gas Flow, % of total Btu
6*
Total Btu/hr x 10
/ft
Oil Flow, GPH
Total Btu integr.
Checker Temp., °F
wo -
Bath Temp., °F
Oil Press., psig
Oil Flow integr.
27*772.
<>„ at NeiLli Biiayuuaii
oe-st
ConiDent8t
'/
782
-------
OPERATING DATA
Location 14
Open Hearth
Taat No.
11' 3
i-3
11'-*
Data
Tina
13:00
13:30
Gas Plow (efh x 1000)
75~
17
IS
77
9*
Purn. Praaa., 'in. H.O
+ U5-
*/,/
Air Flow, (Ota) x 10
2? -30
Oxvaan Plow, (cfh) x 10
ft
7*
?7
Oxvaan Plow intaor.
ftstt
ftf/.f.
Atom.
Plow,- Ifo/hr •
Atom. Staam intaor.
: 7
3f?7. 7
Atom. Staam, Ib/gal aatpoint
Gaa Plow. % of total Btu
to
£0
Total Btu/hr x 10
Iff
Oil Plow. GPH
feo
Total Btu intaar.
. y
Chaekar Tamp.. *P
Ifeo-MW
Iff 0-1120
if 5-9 -mo
Bath Tamp., *P
Oil Praia., paia
75-
Oil Plow intagr.
6. at North Bridgawall
00 at North Brldgewall
Timo of MaaauramantB at
North Bridgewall
Oommentai
FMISH
/{!«'
FtMH if. re
T*r*L 3.
Vt% H»r
111!
Vi
VD
*
fi
I
783
-------
OPERATING DATA
Location 14
Open Hearth
Test No.
Date
Tine
Gas Flow (cfh x 1000)
Furn. Press., in. H_O
za
Air Flow, (cfm) x 10
Oxygen Flow, (cfh) x 10
Oxygen Flow in tear.
Atom. Steam Flow, Ib/hr
Atom. Steam inteqr.
Atom. Steam, Ib/gal setpoint
Gas Flow, % of total Btu
Total Btu/hr x 106
Oil Flow, GPH
Total Btu inteqr.
Checker Temp., °F
Bath Temp., °F
Oil Press., psig
Oil Flow inteqr.
0, at North Bridgewall
CO at North Bridgewall
Time of Measurements at
North Bridgewall
H-3
H-23-76
15'-*'
£2-
1-J.t
23-25-
ffi
tffr.j-
—
?6gf. f
?,(>
?'
i^f
V00
2?f?. f
/70O'f{e
2*fr@l'/:5t>
ie>
•}0f£>00
Comments:
784
-------
OPERATING DATA
Location 14
Open Hearth
Test No.
Date
) -2*1-7?
-11 -7?
3-21-77
t'21-77
Time
Gas Flow (cfh x 1000)
Furn. Press., in. H..O
Air Flow, (cfm) x 10J
Jo
Oxygen Flow, (cfh) x 10
If
If
67
Oxygen Flow integr.
/75V.
Atom. Steam Flow, Ib/hr
(to*
3700
Atom. Steam integr.
7S8?
Atom. Steam, Ib/gal setpoint
t,*
Gas Flow. % of total Btu
ff
Total Btu/hr x 10
/•/£>
Oil Flow, GPH
3?*
370
Total Btu integr.
Checker Temp., "F
2 ore
2-/00
Bath Temp., »F
2.630
Oil Press., psig
3?
//£>
Oil Flow integr.
17717?
172 ?00
P.. at North Bridgewall
7,0
CO at North Bridgewall
Time of Measurements at
North Bridgewall
Coomentst T*rAL
STAtT
3?? re*>S (20%
rtfrji.)
fig 000 &•
HO
Her
-ff?
10: ft
•to:*?
, .
*
J. 0% 03.j2.
p£.
C6>.
ffer
785
-------
OPERATING DATA
Location 14
Open Hearth
Test No.
Date
Tims
Gas Flow (cfh x 1000)
Furn. Press., in. HO
Air Flow, (cfm) x 103
Oxygen Flow, (cfh) x 10
Oxygen Flow integr.
Atom. Steam Flow, Ib/hr
Atom. Steam integr.
Atom. Steam, Ib/gal setpoint
Gas Flow. % of total Btu
Total Btu/hr x 106
Oil Flow. GPH
Total Btu integr.
Checker Tens; . . *F
Bath Temp. . *F
Oil Press., psig
Oil Flow integr.
0. at itecth Bridgewall
CO at North Bridgewall
Time of Measurements at
North Bridgewall
fAf£//AiJ*
P~J£ frff*&
3-21-7?
12: 30
ff
+'f/5"
30
7Z
tHI. 1
3(5"°
fflf€'1
6.0
$-g
/If
38O
1/J*
2>5-0
—
/0y
47S712
3 -21' 77
l?:c>e
0
,t/r
21'f
/$£
/4fV. f
1*00
7#f1
7,1
f~1
?<{
330
I/ 3X> 3
2o?0
2-7/0
Iff
1?g#35~
1.0
3-31-77
I7'30
ft
./J
7*
/e>i
/ff£, 1
fS"*f
7810. 9
7.y
fjf
tjf
3£0
1S39.1
3*19
2$/ 6
t/1
i?fify~
2.0
y -3 1-77
/•ft 00
4f
.'J5~
3?
3-21- 77
If. 30
1 1
* ./0$~
2-f
O
/Q 70.3
2 f&&
7f1?* 7
f.f~
S0
t?0
J20
1/M. /
2.0 /O
—
ft
171W1
Comments i /2 '.33 6AS
12 '•)£ "0
786
-------
OPERATING DATA
Location 14
Open Hearth
Test No.
Date
Time
Gas Flow (cfh x 1000)
Furn. Press., in. HO
Air Flow, (cfm) x 103
Oxygen Flow, (cfh) x 10
Oxygen Flow integr.
Atom. Steam Flow, Ib/hr
Atom. Steam integr.
Atom. Steam, Ib/gal setpoint
Gas Flow, % of total Btu
Total Btu/hr x 106
Oil Flow. GPH
Total Btu integr.
Checker Temp., °F
Bath Temp. , °F
Oil Press., psig
Oil Flow integr.
O, at North Bridgewall
CO at North Bridgewall
Time of Measurements at
North Bridgewall
M&t/M£
2-21-77
/5;00
0
-, 0g-
6
0
1170. 3
/S~00
?f0.f
?>g
f0
f23
?30
l/fS. 3
/17*
• —
7f
7#00/J.
Comments t ffl0l p tfiMf/ffff £0/tTlA)£ f(/£^AC£
tow
lf.lt
3*7
tit
787
-------
OPERATING DATA
Location 14
Open Hearth
Test Ho.
Date
Time
Gas Flow (cfh x 1000)
Furn. Press. ( in. HO
Air Flow, (cfm) x 103
Oxygen Flow, (cfh) x 10
Oxyqen Flow inteqr.
Atom. Steam Flow, Ib/hr
Atom. Steam inteqr.
Atom. Steam, Ib/gal setpoint
Gas Flow. % of total Btu
Total Btu/hr x 106
Oil Flow, GPH
Total Btu integr.
Checker Temp., °F
Bath Temp. , °F
Oil Press., psicr
Oil Flow inteqr.
On at North Bridgewall
CO at North Bridqewall
Time of Measurement! at
North Bridgewall
gMfl/ȣ
3-34-77
17'- '20
(3
+ .61
2- f
S-7
>171. J
Z000
•?f00. 3
*'g
*0
/?•(
3*0
Itff. 2
/
-------
OPERATING DATA
Location 14
Open Hearth
Test No.
Date
Tine
Gas Flow (cfh x 1000)
Purn. Press. , in. HO
Air Flow, (cfm) x 103
Oxygen Flow, (cfh) x 10
Oxygen Flow integr.
Atom. Steam Flow, Ib/hr
Atom. Steam integr.
Atom. Steam. Ib/gal setpoint
Gas Flow, % of total Btu
Total Btu/hr x 106
Oil Flow, GPH
Total Btu integr.
Checker Temp., *F
Bath Temp., °F
Oil Press., psig
Oil Flow integr.
0. at North Bridgewall %
CO at North Bridgewall %
Time of Measurements at
North Bridgewall
l*«/ ~
?fY0.2
?'(
£0
120
??f
32*1.2.
30*0
—
HI
3ftf25~
O
1.0
ItfO
7-70-77
1:20
fT
+.1/5-
30
£1
2oty.-3
11
7112-1
f
I*.?
fffgei
TXAce
f.r
W
3-?o~ 7?
/0:00
0
•t-.wr
23
tit
20/13-
2$~
7fff'/
£
f0
#2-
0
122f
2-tOO
2 fir
2*0
7Ptf02.
f.f
fuff. eff
//;/*
3 -30 -77
/0:?e>
73
•t-.n
*s~
0
3-011
37
71V f.t
7
S0
/23
370 o
9-2-Z
0
PffAS OPfU
^^
^-^^
2-30-77
//:0o
0
+-,02.
r
-------
OPERATING DATA
location 14
'Open Hearth
Test Ho.
Date
7-50-77
2-30-77
Time
12:00
Gas Flow (cfh x 1000)
HI
lit
77
Furn. Press., in. H_0
i-0,/1
Air Flow, (cfm) x 10J
21
Oxygen Flow, (cfh) x 10
28
Oxygen Flow integr.
2020.1
2021
2 022. 0
Atom. Steam Flow, Ib/hr
if
5-1
2?
Atom. Steam integr.
71 f-
Atom. Steam, Ib/gal setpoint
7,7
Gas Flow, % of total Btu
£0
Total Btu/hr'x 10
Oil Flow, GPH
300
Total Btu integr.
1230. 3
, 2.
423*?. 2-
Checker Temp., "F
2-000
Bath Temp., "F
Oil Press., psig
/Vo
Oil Flow integr.
1*5-2
1*^72
O, at North Bridgewall
CO at North Bridgewall
Time of Measurements at
North Bridgewall
13 -
Comments:
13.: 03-
12-37
«?/«/ (?
G J
POO KS.
TOTAL t/£AT 735,0007?:
10
sour* rt«f
fo
7 <
. If *t£C£SS*/eY Tf/£
/*
/J
790
-------
OPERATING DATA
Location 14
Open Hearth
Test No.
Date
3-30-77
J-fr-77
Tine
Gas Plow (ofh x 1000)
13
Furn. Press., in. H.O
*-.//
Air Flow, (efm) x 10J
Oxygen Plow, (ofh) x 10
y-7
ft
Oxygen Plow inteqr.
Atom. Steam Flow. Ib/hr
if
Atom. Steam inteqr.
7W.3
71*2-5-
Tiff. 1
Atom. Steam. Xb/gal eetpoint
i.f
1.*
Cas Plow. % of total Btu
ft
fff
Total Btu/hr x 10°
/5V
Oil Plow. CPH
370
SI*
370
370
Total Btu intern.
. f
Checker Temp., *P
3/00
212-0
Bath Temp.. *F
Oil Press., paig
9 1
31
Oil Flow integr.
0. at North Bridqewall
CO at North Bridqewall
Time of Measurements at
North Bridgewall
Comaentsi
If: It
:/f-'i./f
If'.Zf
, 2
Off # re
Af0/rfi/£S.
79 1
-------
LOCATION 14
Fuel Gas Chromatographic Analysis
Nitrogen
Oxygen
Carbon Dioxide
Carbon Monoxide
Hydrogen
Methane
Ethane
Propane
C 4
C 5
C 6
Heating Value (calculated)
35.2% (by volume)
S.54
0.42
< 0.05
< 0.1
54.4
1.22
0.15
0.056
0.034
0.015
580 BTU dry/SCF
792
-------
LOCATION 14
Fuel Oil Analysis
Carbon,.% 85.62
Hydrogen, % 11.60
Nitrogen, % 0.29
Sulfur, % 1.06
Ash, % 0.045
Oxygen (by difference), % 1.39
API Gravity at 60°F 17.4
Gross Heat of Combustion, BTU/lb 18,640
Net Heat of Combustion, BTU/lb 17,580
793
-------
Test No..
No.
PAKTICULATE EMISSION CALCULATIONS
7f Location /"/
Engr.
Fuel W /64S Sampling Train and Method
Pi tot Factor, Ft
Barometric Pressure, P.
.
in. Hg
Tot. Liquid Collected, V
Velocity Head, A
Sample 'Volume, V
ml Total Particulate, M Hi* • 3 m gm
Stack Temp., Ts W7 *R stack Area, As_/
ft
ft stack Press., P»q
ing Excess
, X0a%
Orifice Press, oiff., H &• 72- iwg Stack Gas Sp. Gravity, Gs
Sample Tine, 6 120 min Nozzle Dia., Dn 0,2-f in. Meter Temp., T
*1. Sample Gas Volume Vm>td - 0.0334 Vm(Pw_^ + H/13.6)
n.d.
Vw . . - 0.0474 V.
sta 1C
2. Water Vapor
3. Moisture Content Bwo • Bq. 2/(Bq. 1 «• Eq. 2)
'std
4. Concentration a. C - 0.0154 Mn/Vn
b. C - 2.205 x 10~6 Mn/Vm
o. C • Eq. 4b x 16.018 x 10
5. Abs. Stack Press. Ps - Pbfcr x 13.6
std
3
6. Stack Gas Speed Vs - 174 Fs /SPTs yjj*- x ~p
7. Stack Gas Flow a. Qsw • Bq. 6 x As x =— x 7^7
Rate 0 70*F •'
b. fisd • Eq. 7a x (1. - Bq. 3)
8. Material Flow Ms • Eq. 7b x Eq. 4b x 60
XOjf - 2090/(20.9 - X02%)
10. Emission a. E • Bq. 4b x Fe x Eq. 9
b. E • Eq. 4c x Fm x Bq. 9 x 1000
9. X02 factor
11. % Isokinetic
14077 x Ts(Vm ,. + VW
— s1
8 x Vs x Ps x Dn
Fe SC Feet/104 Btu
Fm SC Maters/104 joules
Oil
92.2
0.002475
Gas
87.4
0.002346
Coal
98.2
0.002636
3't?
SCF
SCF
grains/DSCF
grams/DSCM
1020. ff
> 7 in. w aes.
ft/min
wsCF/min
DSCF/min
-------
DHIOOIOM CALCULATIONS
Test No.
Unit No.
- 2.
Pitot Factor, Fs
Date Jl-/f-7f Location XV 0&*J
Fuel 0H- + #G Sampling Train and Method
O.
Engr.
Barometric Pressure, P. 30,3 '
Tot. Liquid Collected, V
ml Total Particulate,
_in. Hg
t
m gm
Velocity Head, AP__-_?/£__iwg Stack Temp., Ts_f££__eR Stack Area, As ^ f ft2
Sample Volume, Vm i/2.?/2 ft3 stack Press., psg - 57 5~ jyg Excess O , XO t / ?. 7g 7 wsCF/min
DSCF/min
N.D.
Ib/MMBtu
12-2. I ng/joule
•Multiply Vm . by 530/T (°R) if meter not temp, compensated.
8td ID
Data Sheet 6002-4
795
-------
Test Ho.
Box Mo.
Test Description
PARTICUIATE CALCULATION SHEET
Date !1~WU-7f Location /_
Sample Probe Position
Test Crew
Dry Gas Meter Vol. (
Final
Initial
Total
Beaker No. /
Date
Weighed /? ^OV 7*
Tare 1 loo.01Xi
Wt. 2i0o.018f
3 ^
4
5
6
Km"l0*-0ft'f
Bottle No. '
Impinger
Content (Water)
Rinse (ml) f^^
Date Weighed
or 250 Bake
Final \\oo.ni3
Wt. 250 2100.1315
3
Initial It
A Vol '/
1
11, 2 f 77
If. 2f77
\s
11. 2f77
3
Probe
(Water)
200
1?. 2- $75'
11, 2X75'
is
ej tf,.2 g"?f
.'US
7
101.01(7
lo^.oif 7
S
lei- */f7
.***•
Impinger
1 2
0 II V
0 100
f if
f
1f.W2
1g.f?i3.
^
IV.qjfy.
H
Cyclone
(Acetone)
*J00
13' Ifff
11. If If
!^'
11. /5V £
0.^7-i
*f*tu**m
11.337!
11.3372.
^
lot. f ?5"/"
/et.y&fr
,/
inc. ft??
Flask
(Dry)
102.32*7
102. 12 ft
i/
I02.3J.?7
l.ti'2.
AW/"?
If. 3V IF
??-3<4}g
^
11.313%
.**«
>1 (ml)
S. Gel 1
£ t£. 1 1
£?J. ? /
/3--1 I
Filter
No.
12-
,gff2f
. gez 6
tS~
.103.6
3.,7l/5f>
2.,7fH 1
^
2-7V11
1.1 W
\jtal
'y
-------
PLANT
LOCATION
OPERATOR"
DATE
METHOD 5 CONTROL CONSOLE READINGS
.11
RUN NO.
SAMPLE BOX NO^T
METER BOX NO. ~~T
1ETER H
z FACTOR"! 7W
AMBIENT TEMPERATURE
BAROMETRIC PRESSURE "
ASSUMED MOISTURE, % "
HEATER BOX SETTING "
PROBE LENGTH, IN.
NOZZLE DIAMETER, IN."
PROBE HEATER SETTING"
SCHEMATIC OF STACK CROSS SECTION
Traverse
Point
Number
TOTAL
WCRAPH
Sampling
Time
(o)Min.
CLOCK
rtfit
t22.f
12-
op
^
ff
re>
rt
f*
S2
6?
£t
ft
AVG.
wr. .
Sample
Box
remprta-
ture
Op
}00
3F
AVfi.
Temperature
of Gas
Leaving
Condenser on
jast Impinger
op
V0
V*
V7
yy
y^
f/
v/
<-/!
w
-
CO
-------
Test No.
TEST RUN NO. /V " 3
IMPACTOR NO. /
CASCADE IMPACTOR DATA SHEET
LOCATION
DATE
CYCLONE NO.
OPERATOR
/?.
fruc-
SAMPLE POINT LOCATION
SUBSTRATE COATING \IAAJ ^
FUEL
TEST LOAD
IMPACTOR ORIENTATION
FLOW THRU IMPACTOR
.klb/hr
CFM
FLUE STATIC PRESSURE ~~Si$ inH,0,VELOCITY
V mm IMPACTOR PRESSURE DROP
NOZZLE DIA.
GAS METER END
END TIME
CF
CF
GAS METER START ,
GAS VOLUME /. It ± CF
AMBIENT TEMPERATURE
FLUE GAS MOLECULAR V
START TIME
DURATION
/ &^ t i
FLOW RATE
CFM
_*F PRESSURE 3 O, 7/ IN Hg. HUMIDITY "—" %
_, TEMP. W Q *F , DENSITY 0> ~?J3g/cc .VISCOSITY POISE
Foil + Sample, g
Unused Foil, g
Sample, g
Correction
for Blank, g
Final Sample, g
Stage Number
1
3.6^99
3.67J7
2
1Z6V>
*z.**>
.#>vy
3
1.«c?i
3.^V
4
3. W50
i^75-
,^?r
5
3. 7^6
i74f5'
Stage
Blank
FILTER NO.
Sample Blank
FILTER + SAMPLE, g
FILTER TARE, g
SAMPLE, g
CORRECTION FOR
BLANK, g
FINAL SAMPLE, g
f>. 77M
FULL CONTAINER, g ff,
EMPTY CONTAINER, g 0,
CYCLONE CATCH, g 0,
708
60-20
-------
VELOCITY TRAVERSE
T««t Description!
B«t«i
loc*tioni_
ODitl
'*Mtt
•tack Ores* Motion
Personneli
Barometric Preie. (in. 89)1
Absolut* Static Preie. in Stack (in. Bg) i_
Pitot Tub* Coutfleiuti
(P.)
1/2
Tin*
Tr*v«rM Point
Port Depth
*»Vk
12.
21
3f
HI
ff
7*
M6 -
Velocity
Head
(in. ^jO)
AP
,Vi
.ya ,
.31
.3f
.3?
,3?
.3*5-
CM ftqp.
CP)
vf*
>
j
Oat T»np.
(•»)
*fi
r
Nolccultr
Nt.
MS
Velocity
(ft/seef
VS
1
i?.g
Oj
Cone.
(% Dry)
600J-13
799
-------
TRACE SPECIES AND ORGANICS SAMPLING CONDITIONS
OPEN HEARTH FURNACE - LOCATION 14
Test Number .
Date
Port Location
Velocity, m/s (f/s)
Stack Temp., K (°F)
Oxygen Content, % dry
Moisture, %
Sample Time, rnin..
Cyclone Flow, awm /m (awcfm)
Isokinetic Rate, %
Oven Temp., K (°F)
XAD-2 Temp., K (°F)
Meter Temp., K (°F)
Nozzle Size, mm (in.)
No. of Filters Used 3
Sample Flow, dry, DNm /m (scfm)
Volume Collected, dry, DNm3 (scf)
Particulate Collected, g
Solid Particulates, ng/J (Ib/MMBtii)
Unit Conditions
Test Time, min.
Process Rate, tons/cycle
Hot Metal/Scrap, %/%
Fuel '
Fuel Flow Rate, g/s (Ib/hr)
Stack Flow Rajte, Nm3/s (SCFM)
14-2
11-18-76
ESP Inlet (sample point A)
13.96 (45.8)
522 (480)
13.9
6.9
164.6
0.1226 (4.33)
106
463 (373)
295 (71)
294 (70)
14.3 (0.562)
2
0.073 (2.56)
11.95 (421.9)
22.806
1372 (3.19)
230
375
48/52
Natural gas and No. 6 oil
402 (3200)
48.3 (102300)
800
-------
Project:
Date:
PffA$£ M
KVB, INC. TRACE SPECIES AND ORGAN ics SAMPLING DATA
PtVJftTA,*46f*TY
Personnel: /fe£X//*/g. MM/AlG Barometric Press »
. /f. 117*
Location:
Unit: m -
Test: ',
! Mr. £AS +
Probe Nozzle Diameter (inches)i
Absolute Static Press, in Stack (in. Hg)t
Pitot Tube Coefficienti
_(Dn)
_(Ps)
_(Cp)
T I
Real
4 B
Elapsed
Traverse
Point
Depth
Pitot
AP
(in H20)
Orifice
AP
(in H20)
Cum.
Meter
Volume
(ft3)
Pump
Suction
(in. Hg)
TEMPERATURE (*P)
Stack
Probe
XAD-2
Impinger
Out
Oven
Meter
£n/Out
Cone.
% dry
.3?
V*
371
If
#02.
.Vf
1.3
63
3*7
ff
rt
CO
167.000
ff.0
$-02.
£2.
Ft
Y5-
I2--0
372-
7f
IjfO
5-3
i/i
72.
72-
ff
7t
{0
iff
77
7f
/Y'2-
£7
rr
77
77
Hii
1Z2-
37?
77
1*3
3*3
It
r*
IW1
.ff
fto
Iff!
127.3
.VH
3.0
It oo
1*7.3
J.3
7/f.ZOO
71
7*
1*30
1*7,3
3.3
17.3-
1637
tt.F
-------
TRACE SPECIES AND ORGANICS TEST
SAMPLE RECOVER* LOG
Tut MO.
Data
Saqple Port Position
location i4 - Ot»c-t.l yeAJCTi
a OF!*.
Container
Nunfcer
SSfc
514.
Sfeft
432:
t*
felS
532:
.430.
6R
Saaple Description
S • T ji
&M.ICS
Tk-T
S
L T> 4-Vl
I
-Wpt 5
Container
Type
us.
Ret
wt/vol.
4l4.(
tA4td
SoU
Coiiiuent .
Kns-7ig.aaal
802
-------
TRACE SPECIES AND ORGANXCS TEST
SAMPLE RECOVERY LOG
Teat No.
Oat*
location
iie*gT4 ToeUA.CC
Sample Port Position
VJg
\4-
Vfc
\4U
Container
Number
S6A
52.Z
fltjQ
Saqple Description
T> 4- Vi 4-
T
jX
luo
\pc<
N
Container
Type
Ik
V!fcp<
Net
wt/vol.
SAM.
IJlS
Comment-
is*.
loo^g
toofe
ses
Data Sheet KVB 6002-15
803
-------
14-Open Hearth Furnace
Test 14
TABLE upstream of Precip.
POLLUTANT
SAMPLE NUMBER
Antimony
Arsenic
Barium
Beryllium
Cadmium
Calcium
Chromium
Cobalt
Copper •
Iron
Lead
Manganese
Mercury
Nickel
Selenium
Tellurium
Tin
^
Titanium
Vanadium
Zinc
Chloride
Fluoride
Nitrates
Sulfates
556+
-IS
2.0
/3o
32-0
-------
14-Open Hearth Furnace
Test 14 TABLE upstream of Precip.
POLLUTANT SAMPLE NUMBER
Antimony
Arsenic
Barium
Beryllium
Cadmium
Calcium
Chromium
Cobalt
Copper
Iron
Lead
Manganese
Mercury
Nickel
Selenium
Tellurium
Tin
Titanium
Vanadium
Zinc
Chloride
Fluoride
Nitrates
Sulfates
L*
O.S
•<«
<-\
*o./
O.JS
1.V0
33. s
5.3t
nsoo
L* dupl
o.s
<:o.o,o
-------
14-Open Hearth Furnace
Test 14 TABLE Upstream of Precip.
POLLUTANT SAMPLE NUMBER . .
Antimony
Arsenic
Barium
Beryllium
Cadmium
Calcium
Chromium
Cobalt
Copper
Iron
Lead
Manganese
Mercury
Nickel
Selenium
Tellurium
Tin
Titanium
Vanadium
Zinc
Chloride
Fluoride
Nitrates
Sulfates
682*
.-?,
Ho
<0.io
.oos
<£0.0/
o./o
^»O*O^^7
\-2.
^o-l
• \\
<\
<2.S
<^s
li!oP
<2S
-------
COMMERCIAL TESTING & ENGINEERING CO.
•CNt*Ai ernotii itt MOUTH LA SALLC cricrr. omo»ao. ILLINOIS so*oi • AHA coot in M*-t4i4
Reply tO IMTMMUNTM ANALYSIS DIVISION, 14H5 WtST *»TH AVIMUI, OOIOCN. COIOIAOO SMOI, PHONI, XMTMfll
Te> Mr. John G. M1cha1ov1c ^Ji^.
Calspan Corporation ^^5.»»
Post Office Box 235
Buffalo, NY 14221
Date: April 23, 1977
Analyst: S. Sweeney
P. O. No.: 27810
Sample No.:
Test 14 A
556, 574, 568
, 290. 461
IAD No.:
97-A197-134-31
CONCENTRATION IN PPM WEIGHT
ELEMENT
Uranium
Thorium
Bismuth
Lead
Thallium
Mercury
Gold
Platinum
IMdlum
Osmium
Rhenium
Tungsten
Tantalum
Hafnium
Lutetian
Ytterbium
Thulium
Erbium
Hoi ml urn
Dysprosium
CONC.
17
22
2
210
28
NR
10.1
7
<0.8
0.5
0.3
2
0.4
2
3
5
ELEMENT
Terbium
Gadolinium
Europium
Samarium
Neodymlum
Praseodyml urn
Cerium
Lanthanum
Barium
Cesium
Iodine
Tellurium
Antimony
Tin
Indium
Cadmium
Silver
Palladium
Rhodium
CONC.
1
3
2
6
26
12
91
49
MC
4
6
<0.7
23
24
STD
3
5
ELEMENT
Ruthenium
Molybdenum
Niobium
Zirconium
Yttrium
Strontium
Rubidium
Bromine
Selenium
Arsenic
Germanium
Gallium
Z1nc
Copper
Nickel
Cobalt
Iron
Manganese
Chromium
CONC.
53
27
100
39
760
200
45
36
98
66
78
MC
320
110
36
MC
MC
540
ELEMENT
Vanadium
Titanium
Scandl urn
Calcium
Potassium
Chlorine
Sulfur
Phosphorus
Silicon
Aluminum
Magnesium
Sodium
Fluorine
Oxygen
Nitrogen
Carbon
Boron
Beryllium
Lithium
Hydrogen
CONC.
220
MC
15
MC
MC
440
MC
MC
MC
MC
MC
MC
"160
NR
NR ,
NR
MC
0.8
33
NR
NR - Not Reported
All elements not reported
<0.1 ppm weight
Approved:
807
-------
COMMERCIAL TESTING & ENGINEERING CO.
GENERAL OFFICES: III NORTH LA IALLE STREET, CHICAGO, ILLINOIS SOSOI • AREA CODE Sll Jt«-i4»4
Reply tO INSTRUMENTAL ANALYSIS DIVISION. 14335 WEST 44TH AVENUE. OOLDEN. COLORADO'«0«01. FHONEi MM7S4511
To: Mr. John G. Michalovic
Calspan Corporation
Post Office Box 235
Buffalo, NY 14221
P.O. No.: 27810
Sample No.: 14 g #1
Date: April 23, 1977
Analyst: s. Sweeney
IAD No.: 97-A197-134-31
CONCENTRATION IN PPM WEIGHT
ELEMENT CONC.
Uranium
Thorium
Bismuth
Lead <1
Thallium
Mercury NR
Gold
Platinum
Irldlum
Osmium
Rhenium
Tungsten
Tantalum
Hafnium
Lutetlum
Ytterbium
thulium
Erbium
Holmlum
Dysprosium
ELEMENT CONC.
Terbium
Gadolinium
Europium
Samarium
Neodymium
Praseodymi urn
Cerium
Lanthanum
Barium 5
Cesium <0.1
Iodine
Tellurium
Antimony
Tin
Indium STD
Cadmium
Silver 12
Palladium
Rhodium
ELEMENT
Ruthenium
Molybdenum
Niobium
Zirconium
Yttrium
Strontium
Rubidium
Bromine
Selenium
Arsenic
Germanium
Gallium
Zinc
Copper
Nickel
Cobalt
Iron
Manganese
Chromium
CONC.
4
2
0.3
2
0.1
1
0.5
<0.3
0.3
5
2
2
<0.1
67
0.4
9
i /
ELEMENT
Vanadium
Titanium
Scandium
Calcium
Potassium
Chlorine
Sulfur
Phosphorus
Silicon
Aluminum
Magnesium
Sodium
Fluorine
Oxygen
Nitrogen
Carbon
Boron
Beryllium
Lithium
^Hydrogen
CONC.
0.3
16
<0.09
110
480
3
14
27
800
120
15
99
K3
NR
NR .
NR
7
0.2
NR
NR - Not Reported
All elements not reported <0.3 ppm weight
Total sample was Inadvertently ground in a
Approved:
coors mortar'4'pesfl^
See attached note.
808
-------
Reply to
COMMERCIAL TESTING & ENGINEERING CO.
tttNtHAl OmCtt: t«« MOUTH IA (M.IC »T«tT, CHICABO, IU.INOI* (0*01 • AtlA OOO« til tt«-»«»4
INSTIUMtMTAl ANA1TSU DIVISION. I4JJJ WU1 44TN AVINUI. COIDCN. COlOtAOO KMOI. PHONIi MU7MI1I
To: Mr. John Mlchalovlc
Calspan Corporation
Post Office Box 235
Buffalo. NY 14221
P.O. No.= 27810
Sample No.: 14 B 12
D.te: April 23, 1977
Analyst: S. Sweeney
IAD No.: 97-A197-134-31
CONCENTRATION IN PPM WEIGHT
ELEMENT CONC.
Uranium
Thorium
Bismuth
Lead
hour 1n a laboratory
ELEMENT
Vanadium
Titanium
Scandium
Calcium
Potassium
Chlorine
Sulfur
Phosphorus
Silicon
Aluminum
Magnesium
Sodium
Fluorine
Oxygen
Nitrogen
Carbon
Boron
Beryllium
L'lthlum
i Hydrogen
f A
ro^t^
furnace In a
CONC.
<0.1
1
-------
Reply tO
COMMERCIAL TESTING & ENGINEERING CO.
•INIIAl OFFICM: 111 NOHTM LA lALlt 1TRIIT, OMIOAOO, IlLINOII «0«0t • AHA CODt III TII-MI4
IMTtUWINTAl ANAinit DIVIIION. I4WS WIST 44TM AVINUI. OOIDIN. COlOtAOO IMOI. MMNIi MM7I491I
Te: Mr. John G. Mlchalovlc Ail^L
Calspan Corporation — —
Post Office Box 235
Buffalo. NY 14221
Da,.: April 22, 1977 '
Anilytt: S. Sweeney
P. O. No.: 27810
Sample No.:
ELEMENT
Uranium
Thorium
Bismuth
Lead
Thallium
Mercury
Gold
Platinum
Ir1d1um
Osmium
Rhenium
Tungsten
Tantalum
Hafnium
Lutetlum
Ytterbium
Thulium
Erbium
Hoi ml urn
Dysprosium
KVB 14 C 616, 268, 671, 677. 672
480, 687 CONCENTRATION
CONC. ELEMENT CONC.
Terbium
Gadolinium
Europium
<0.02 Samarium
Neodymlum
NR Praseodymium
Cerium
Lanthanum
Barium 0.09
Cesium
Iodine 0.02
Tellurium
Antimony
Tin
Indium STD
Cadmium <0.006
Silver MC
Palladium
Rhodium
. 683,
IN yq/ml
ELEMENT
Ruthenium
Molybdenum
Niobium
Zirconium
Yttrium
Strontium
Rubidium
Bromine
Selenium
Arsenic
Germanium
Gallium
Zinc
Copper
Nickel
Cobalt
Iron
Manganese
Chromium
IAD No.:
CONC.
0.9
0.03
0.02
0.08
iO.Ol
<0.002
<0.003
->0.2
0.2
6
0.003
MC
0.2
9
97-A197-134-31
ELEMENT
Vanadium
Titanium
Scandium
Calcium
Potassium
Chlorine
Sulfur
Phosphorus
Silicon
Aluminum
Magnesium
Sodium
Fluorine
Oxygen
Nitrogen
Carbon
Boron
Beryllium
Lithium
yHvdrogen
CONC.
0.003
0.04
<0.001
6
5
0.3
MC
3
1
0.1
0.2
3
«0.3
NR
NR .
NR
0.03
-------
COMMERCIAL TESTING & ENGINEERING CO.
OENEHAl OFFICE*: *!• NORTH LA (ALLE IT»EET, CHICAQO, ILLINOIt IDtOI • AREA CODE III 7H-14I4
Reply to i INSTWMINTAL ANALYSIS DIVISION. i4»s WIST MTH AVENUI, GOLDEN. COLORADO IMOI. WONI.
Mr. John G. Michalovic
Calspan Corporation
Post Office Box 235
Buffalo, NY 14221
P. O. No.: 27810
Sample No.: 14 D #1 1031
Date: April 23, 1977
Analyst: s. Sweeney
IAD No.: 97-A197- 134-31
CONCENTRATION IN PPM WEIGHT
ELEMENT CONC.
Uranium
Thorium
Bismuth
Lead 1
Thallium
Mercury NR
Gold
Platinum
. i . ••
Iridium
Osmium
1 F ,
Rhenium
Tungsten
Tantalum
Hafnium
Lutetlum
Ytterbium
Thulium
Erbium
Holmium
Dysprosium
ELEMENT CONC.
Terbium
Gadolinium
Europium
Samarium
Neodymi urn
Praseodymi urn
Cerium
. Lanthanum
Barium 1
. Cesium
Iodine
Tellurium
Antimony
Tin
Indium STD
Cadmium 1.0.4 .
Silver £0.3
Palladium
• J
Rhodium
_
ELEMENT
Ruthenium
Molybdenum
Niobium
Zirconium
Yttrium
Strontium
Rubidium
Bromine
Selenium
Arsenic
Germanium
Gallium
Zinc
Copper
Nickel
Cobalt
Iron
Manganese
Chromium
CONC.
7
2
0.4
0.9
0.1
<0.2
2
1
10
<0.1
**49
0.3
0.6
ELEMENT
Vanadium
Titanium
Scandium
Calcium
Potassium
Chlorine
Sulfur
Phosphorus
Silicon
Aluminum
Magnesium
Sodium
Fluorine
Oxygen
Nitrogen
Carbon
Boron
Beryllium
Lithium
/Hydrogen
CONC.
16
1
0.3
40
22
4
160
5
**72
**4
8
13
=2
NR
NR
NR
2
0.4
* NR
NR - Not Reported
All elements not reported <0. 3ppm weight Approved
**Heterogeneous -Sample was thermally ashed @ 350°
iw.a ^WM^Z c»veiblo prior to analysis.
ur 1n a laboratory furnace
8 1 1
-------
COMMERCIAL TESTING & ENGINEERING CO.
- SENERAl OFFICE!: 9>S NORTH LA SALLE STREET, CHIOAOO, ILLINOIS S060I • AREA CODE 119 79S-S4S4
Reply to iNstmiMfNTAi ANALYSIS DIVISION, \au WIST UTH AVENUI. GOLDEN, COLORADO tool, FHONI> JOMTSISII
.To: Mr. John 6. Michalovic
Calspan Corporation
, Post Office Box 235
Buffalo, NV 14221
P. O. No.: 27810
Sample No.: 14 Q #2 1031
Date: April 23, 1977
Analyst: s. Sweeney
IAD No:-. 97-A197-134-31
CONCENTRATION IN PPM WEIGHT
ELEMENT
Uranium
Thorium
Bismuth
Lead
Thallium
Mercury
Gold
Platinum
Irldlum
Osmium
Rhenium
Tungsten
Tantalum
Hafnium
Lutetlum
Ytterbium
Thulium
Erbium
Hoi ml urn
Dysprosium
CONC. ELEMENT CONC.
Terbium
Gadolinium
Europium
<0.7 Samarium
Neodymlum
NR Praseodymium
Cerium
Lanthanum
Barium 0.7
Cesium
Iodine
Tellurium
Antimony
Tin
Indium , STO
Cadmium .. <0.3
Silver 0.2
Palladium
Rhodium
NR - Not Reported
All, element* not reported
-------
COMMERCIAL TESTING & ENGINEERING CO.
GEMCVAl OFFICE*: t» NORTH LA 1AILE tTKEET, CHIOA8O, IIIINOI* »0«01 • AUCA CODE tit ?tt-«414
^^eltUMINTAL ANAirill DIVISION. I4J15 WU1 44TH AVINUl. OOIDIN, COlOtADO 10401. FHONI, MM7M331
To: Mr. John Mlchalovic ..fcl^.
Calspan Corporation ^^SK!^^
Post Office Box 235
Buffalo. New York
14221
P.O. No, 27810
Sample No, KVB 14 E 460
Date: April 22, 1977
Analyst! 5. Sweeney
CONCENTRATION IN PPM WEIGHT
ELEMENT CONC.
Uranium <0.8
Thorium
Bismuth
Lead 1
Thallium
Mercury NR
' Gold
Platinum
Iridium
. Osmium
Rhenium
Tungsten
Tantalum :
Hafnium
Lutetlum
Ytterbium
Thulium
Erbium
Hoi mi urn
. Dysprosium
ELEMENT CONC.
Terbium
Gadolinium
Europium
Samarium
Neodymium 0.3
Praseodymium o.l
Cerium o.2
Lanthanum 0.3
Barium 3
Cesium T20
220
>300
"17
NR
NR •
NR
9
!0.3
9
leached in
..__ ^_ i
ultra pure nitric hydrochloric acid shows, rinsed then all
8 1 3
-------
COMMERCIAL TESTING & ENGINEERING CO.
•ENE*AL OFFICE*: It* NORTH LA SALIE STREET, CHIOAOO, ILLINOIt (0*01 • AREA CODE »t< TI*-«4»4
Reply to INSTIUMENTAI ANALYSIS DIVISION. 14BS WEST 44m AVENUE, ooiotN. COIOIAOO w«i. PMONC.
To: Mr. John G. M1chalov1c V*lBiv
Calspan Corporation ^TEJUP^
Post Office Box 235
Buffalo. NY 14221
P. O. No.: 27810
Sample No.: KVB 14 F 479
Dafe. April 22, 1977
Analyst: S. Sweeney
IAD No.: 97-A197- 134-31
CONCENTRATION IN vg/ml
ELEMENT
Uranium
Thorium
Bismuth
Lead
Thai 1 i urn
Mercury
Gold
Platinum
Iridium
Osmium
Rhenium
Tungsten
Tantalum
Hafnium
Utetium
Ytterbium
Thulium
Erbium
Holmium
Dysprosium
CONC. ELEMENT CONC.
<0.03 Terbium
Gadolinium
<0.007 Europium
0.03 Samarium
Neodyrai urn
NR Praseodymi urn
Cerium
Lanthanum
Barium 0.1
Cesium <0.002
Iodine 0.005
Tellurium
Antimony
Tin <0.01
Indium STD
Cadmium <0.007
Silver MC
Palladium
Rhodium
ELEMENT
Ruthenium
Molybdenum
Niobium
Zirconium
Yttrium
Strontium
Rubidium
Bromine
Selenium
Arsenic
Germanium
Gallium
Z1nc
Copper
Nickel
Cobalt
Iron
Manganese
Chromi urn
CONC.
0.2
0.06
0.04
0.01
<0.02
<0.003
<0.003
1
0.'4
0.04
<0.001
0.2
0.009
0.02
ELEMENT
Vanadium
Titanium
Scandium
Calcium
Potassium
Chlorine
Sulfur
Phosphorus
Silicon
Aluminum
Magnesium
Sodium
Fluorine
Oxygen
Nitrogen
Carbon
Boron
Beryl 1 1 urn
Lithium
Hydrogen
CONC.
.0.001
0.03
<0.002
MC
6
0.2
MC
2
0.3
0.4
1
MC
»0.03
NR
NR •
NR
0.01
0.05
NR
NR - Not Reported
All elements not reported <0.004 yg/ltll
Approved:
81 4
-------
COMMERCIAL TESTING & ENGINEERING CO.
R«ply tO
e(Ni*Ai ornotti tn MOUTH LA IALLI »T»I«T, OHIOASO, I'UINOK «o«oi • AHA 0901 *» '
imTMMMNTAl ANAinil DIVIIION. UMJ WUT 44TH AVINUI. OOIOIN, COlOtADO IMOI. fHONIi XM7MS9I
Toi Mr. John G. M1chalov1c ^SlEW
Calspan Corporation —»«•
Post Office Box 235
Buffalo. NY 14221
P. 0. No.. 27810
Simple No.: KVB 14 G 681
Date: April 22, 1977
Analyst: 5. Sweeney
IAD No.: 97-A197-134-31
CONCENTRATION IN pg/ml
» •'
ELEMENT CONC.
Uranium
Thorium
Bismuth
Lead fO.02
Thallium
Mercury NR
Gold
Platinum
IHdlum
Osmium
Rhenium
Tungsten
Tantalum
Hafnium
Lutetlum
Ytterbium
Thulium
Erbium
Holmlum
Dysprosium
ELEMENT CONC.
Terbium
Gadolinium
Europium
Samarium
Neodyml urn
Praseodymium
Cerium
Lanthanum
Barium rj.02
Cesium
Iodine 0.007
Tellurium
Antimony
Tin
Indium STD
Cadmium <0.01
Silver 0.009
Palladium
Rhodium
ELEMENT
Ruthenium
Molybdenum
Niobium
Zirconium
Yttrium .
Strontium
Rubidium
Bromine
Selenium
Arsenic
Germanium
Gallium
Z1nc
Copper
Nickel
Cobalt
Iron
Manganese
Chromium
CONC.
0.2
0.05
0.005
<0.02
<0.003
<0.005
0.09
0.006
0.006
10.001
0.2
0.01
0.007
A
ELEMENT
Vanadium
Titanium
Scandium
Cal c1 urn
Potassium
Chlorine
Sulfur
Phosphorus
Silicon
Aluminum
Magnesium
Sodium
Fluorine
Oxygen
Nitrogen
Carbon
Boron
Beryllium
Lithium
, Hydrogen
CONC.
<0.001
0.02
<0.001
9
0.8
0.2
0.4
0.2
**4
vb.oi
0^2
0.3
«0.2
NR
NR •
NR
0.06
10.001
.NR
NR - Not Reported
All element* not reported
"Heterogeneous
<0.006 yg/ml
Approved:
8 1 5
-------
COMMERCIAL TESTING & ENGINEERING CO.
OENCHAI. OFFICES: ill MOUTH LA SALLE STRICT, CHICA8O, ILLINOIS SOSOI • A»EA CODE 111 T1S-S4I4
Reply tO INSTIUMINTAl ANALYSIS DIVISION. lOiS WCST 44TH AVfNUt. GOIDEN. COIOIADO MMOI. FHONEi XMTMfll
TO! Mr. John G. Michalovic ^CI^L.
Calspan Corporation -«••-
Post Office Box 235
Buffalo, New York
14221
P.O. No.: 27810
Sample No.: KVB 14 H 682
CONCENTRATION IN V9/ml
ELEMENT CONC.
Uranium
Thorium
Bismuth
Lead £0.02
Thallium
Mercury NR
Gold
Platinum
Iridium
Osmium
Rhenium
Tungsten
Tantalum
Hafnium
Lutetium
Ytterbium
Thul 1 urn
Erbium
Hoi ml urn
Dysprosium
ELEMENT CONC.
Terbium
Gadolinium
Europium
Samarium
Neodymium
Praseodymi urn
Cerium
Lanthanum
Barium 0.02
Cesium
Iodine
Tellurium
Antimony
Tin
Indium STD
Cadmium £0.007
Silver 0.006
Palladium
Rhodium
ELEMENT
Ruthenium
Molybdenum
Niobium
Zirconium
Yttrium
Strontium
Rubidium
Bromi ne
Selenium
Arsenic
Germanium
Gallium
Zinc
Copper
Nickel
Cobalt
Iron
Manganese
Chromi urn
Date: April 22, 1977
Analyst: S . Sweeney
IAD No.= 97-A1 97-1 34-31
CONC.
0.1
0.06
0.008
0.008
£0.002
£0.003
o:o6
0.01
0.005
£0.001
0.05
0.002
0.05
ELEMENT
Vanadium
Titanium
Scandi urn
Calcium
Potassium
Chlorine
Sulfur
Phosphorus
Silicon
Aluminum
Magnesium
Sodium
Fluorine
Oxygen
NI trogen
Carbon
Boron
Beryllium
Lithium
Hydrogen
CONC.
0.001
0.01
£0.001
0.7
0.1
0.1
0.4
1
0.4
* 0.009
0.2
0.1
=0.6
NR
NR
NR
0.01
0.006
NR'
NR - Not Reported
All elements not reported <0. 004 fig/ml
"Heterogeneous
Approved:
"8 r b
-------
COMMERCIAL TESTING & ENGINEERING CO.
OCNERAL OFFICE*: I2B NORTH LA (ALII (THECT. CHICAGO, ILLINOII 10(01 • AREA CODE (II Tl»-(4»4
Reply 10 INSTMJMINTAl ANAIYSIS OIVIIION. 14315 WIST 44TH AVINUI. COIOIN. CCiOtADO (MM. PMONIi
To-. Mr. John 6. M1chalov1c ^1^.
Calspan Corporation ^5rJf^
Post Office Box 235
Buffalo, NY 14221
P. 0. No.: 27810
Sample No.: KVB 14 I 678
Date: April 22, 1977
Analyst: S. Sweeney
IADNo.:97_Ai97-i34-3i
CONCENTRATION IN Jig/ml
ELEMENT CONC.
Uranium
Thorium
Bismuth
Lead £0.3
Thallium
Mercury NR
Gold
Platinum
Irldium
Osmium
Rhenium
Tungsten
Tantalum
Hafnium
Lutetlum
Ytterbium
Thulium
Erbium
Hoi ml urn
Dysprosium
ELEMENT CONC.
Terbium
Gadolinium
Europium
Samarium
Neodyml urn
Praseodymi um
Cerium
Lanthanum
Barium 0.4
Cesium
Iodine 0.1
Tellurium
Antimony
Tin <0.2
Indium STD
Cadmium '<0.1
Silver **0.4
Palladium
Rhodium
NR - Not Reported
All elements not reported < 0.008 |*g/m1
^Heterogeneous -Sample was thermally
ELEMENT
Ruthenium
Molybdenum
Niobium
Zirconium
Yttrium
Strontium
Rubidium
Bromine
Selenium
Arsenic
Germanium
Gallium
Zinc
Copper
Nickel
Cobalt
Iron
Manganese
Chromium
Approved: '/
ashed 9 350°
-------
KVB Analysis Data
Sample Number POM's PCB's
298 < 1 ug/g < 1 ug/g
534 < 1 ug/g < 1 ug/g
534 (duplicate) < 1 ug/g < 1 ug/g
13-18 740 90 ug/g < i'ug/g
13-18 282 49 ug/g < l Ug/g
13-18 -530 3.2 ug/g . < 1 ug/g
13-18 1038 6.3 ug/g < 1 ug/g
13-18 1032 396 ug/g < 1 ug/g
13-18 1033 1 ug/g < 1 ug/g
13-18 1034 8 ug/g < 1 ug/g
13-18 1034 (duplicate) 9 ug/g < 1 ug/g
13-24 735 513 ug/g < 1 ug/g
531 6.9 ug/g < 1 ug/g
1039 20 ug/g < 1 ug/g
1035 144 ug/g < 1 ug/g
1036 10 ug/g < 1 ug/g
1037 7.1 ug/g < 1 ug/g
1037 (duplicate) 8.5 ug/g < 1 ug/g
14 556 70.5 ug/g < 1 ug/g
568 104 ug/g < 1 ug/g
532 10.7 ug/g < 1 ug/g
532 (duplicate)- 8.2 ug/g . < 1 ug/g
15-10 1041 <0.1 ug/g <1 ug/g
1041 (duplicate) < 0.1 ug/g < 1 ug/g
. 1042 * *
15-11 941 < 1 ug/1 < 1 ug/1
1044 < 0.1 ug/g < 1 ug/g
1045 * *
19-1 LF * *
19-2 533 <0.1 ug/g <1 ug/g
533 (duplicate) < 0.1 ug/g <1 ug/g
C <1 ug/r~ <1 ug/1
C (duplicate) < 1 ug/1 < 1 ug/1
LF * *
*Sample extracts too concentrated to be able to determine an analytical value,
818
-------
KVB ANALYSIS DATA
-3-
SAMPLE
14 616
POM's
27 ug/1
PCB'S
12/2 - 3 B
12/2 - 6 E
13/18 M
13/18 M deep
13/18 N
13/24 609
13/24 A
'< 10 ug/1
10 ug/1
2480 ug/1
2890 ug/1
225 ug/1
234 ug/1
10 ug/1
' 1 ug/1
'1 ug/1
< 10 ug/1
< 10 ug/1
-------
DIESEL ENGINE
Location No. '5 Unit No.
Unit Description £)\£<5>£.U.
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E- n GJ
Installation Date
Heater Rating
!.£, UO (4-. I >< \O
Burner Description
Test Fuel Combinations
Q\u. C O. ^S %,
Fuel Temp, at Biurner (°F) _ &C| Kl ( |Q)Q°F
Primary Air Temp. (°F) _ ^\. 1^. (_ \ t>, QQT-"
Comments:
820
-------
Unit No.
Unit Type
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MOBILE LABORATORY DATA
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8. Oxygen (%)
9. NOx (hot) read/3% 02 (ppm)
10. NO (hot) read/3% 02 (ppm)
11. NO? (hot) read/3% 02 (ppm)
12. NO (cold) read/3% 02 (ppm)
13. Carbon Dioxide (%)
14. Carbon Monoxide (ppm) uncor/cor
15. Hydrocarbon (ppm) uncor/cor
16. Sulfur Dioxide (ppm) uncor/cor
17. Smoke Spot (Bacharach)
18. Atmos. Temp. (°F/°C)
19. Dew Point Temp. (°F/eC)
20. Atmos. Pressure (in. Hg)
21. Relative Humidity (%)
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12. NO (cold) read/3% 02 (ppm)
13. Carbon Dioxide (%)
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15. Hydrocarbon (ppm) uncor/cor
16. Sulfur Dioxide (ppm) uncor/cor
17. Smoke Spot (Bacharach)
18. Atmos. Temp. (°F/°C)
19. Dew Point Temp. (°F/°C)
20. Atmos. Pressure (in. Hg)
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13. Carbon Dioxide (%)
14. Carbon Monoxide (ppm) uncor/cor
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16. Sulfur Dioxide (ppm) uncor/cor
17. Smoke Spot (Bacharach)
18. Atnos. Temp. (°F/°C)
19. Dew Point Temp. (°F/°C)
20. Atmos. Pressure (in. Hg)
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16. Sulfur Dioxide (ppm) uncor/cor
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18. Atmos. Temp. (°F/°C)
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8. Oxygen (%)
9. NOx (hot) read/3% 02 (ppm)
10, NO (hot) read/3% 02 (ppm)
11. NO? (hot) read/3% 02 (ppm)
12. NO (cold) read/3% 02 (ppm)
13. Carbon Dioxide (%)
14. Carbon Monoxide (ppm) uncor/cor
15. Hydrocarbon (ppm) uncor/cor
16. Sulfur Dioxide (ppm) uncor/cor
17. Smoke Spot (Bacharach)
18. Atitos. Temp. (°F/°C)
19. Dew Point Temp. (°F/°C)
20. Atmos. Pressure (in. Hg)
21. Relative Humidity (%)
22.
23.
24.
25.
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Test No.
Unit No.
MOBILE LABORATORY DATA
Date 4-S9-77 Location
Fuel *C? QS<- Capacity
Test No.
Engr.
?S~ X
Chit Type £>/«£'-
Bumer Type_
1. Test No.
2. Date
3. Time
4. Load X tJ
5. Process Rate
6. Flue Diam. or Size, ft
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9. NOx (hot) read/3% 03 (ppm)*
10. NO (hot) read/3% 02 (ppm)*
11. NO? (hot) read/3% 02 (ppm)*
12. NO (cold) read/3% O2 (ppm)*
13. Carbon Dioxide (%)
L4. Carbon Monoxide (ppm) uncor/cor
*
15. Hydrocarbon Jppm) uncor/cor
16. Sulfur Dioxide (ppm) uncor/cor
17. Smoke Spot (Bacharach)
18. Atitos. Temp. (°F/°C)
19. Dew Point Temp. (°F/eC)
20. Atmos. Pressure (in. Hg)
21. Relative Humidity (%)
22.
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Data Sheet 6002-2
827
-------
MOBILE LABORATORY DATA
Test No._/£V&j5£££_ Date 7j=>"
Test
Engr.
g.)
Onit Type D/£
Burner Type_
1. Test No.
2. Date
3. Time
4. Load K (>J
5. Process Rate
6. Flue Diam. or Size, ft
7. Probe Position
8. Oxygen (%)
9. NOx (hot) read/3% 02 (ppm)*
10. NO (hot) read/3% 02 (ppm)*
11. NO? (hot) read/3% 02 (ppm)*
12. NO (cold) read/3% O2 (ppm)*
13. Carbon Dioxide (%)
14. Carbon Monoxide (ppm) uncor/cor
*
15. Hydrocarbon (ppm) uncor/cor
16. Sulfur Dioxide (ppm) uncor/cor
17. Smoke Spot (Bacharach)
18. A tiros. Temp. (°F/°C)
19. Dew Point Temp. (°F/°C)
20. Atmos. Pressure (in. Hg)
21. Relative Humidity (%)
22.
23.
24.
25.
26.
27.
28.
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the value is measured on a wet basis.
Data Sheet 6002-2
828
-------
MOBILE LABORATORY DATA
Test No. /5~- //' $4 $5 Date 1 "2-/- 7 7 Location
Unit No. Fuel 7££ &/t- Capacity_
Test No.
Engr
Unit Type
.Burner Type
1. Test No.
2. Date
3. Time
4. Load
5. Process Rate
6. Flue Diam. or Size, ft
7. Probe Position
8. Oxygen (%)
9. NOx (hot) read/3% 03 (ppm)
10. NO (hot) read/3% 02 (ppm)
11. NO? (hot) read/3% 02 (ppm)
12. NO (cold) read/3% O2 (ppm)
13. Carbon Dioxide (%)
14. Carbon Monoxide (ppm) uncor/cor
15. Hydrocarbon (ppm) uncor/cor
16. Sulfur Dioxide (ppm) uncor/cor
17. Smoke Spot (Bacharach)
18. Atmos. Temp. (*lEX0C)
19. Dew Point Temp. (°F/°C)
20. Atmos. Pressure (in. Hg)
21. Relative Humidity (%)
22.
23.
24.
25.
26.
27.
28.
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Data Sheet 6002-2
-------
Test No.
Unit No.
MOBILE LABORATORY DATA
Date *f-2f '77 Location /_
Fuel ^^2 &/l~ Capacity_
Test No.
Unit Type
Buzner Type_
1. Test No.
2. Date
3. Time
4. Load
5. Process Rate
6. Flue Diam. or Size, ft
7. Probe Position
8. Oxygen (%)
9. NOx (hot) read/3% 03 (ppm)
10. NO (hot) read/3% 02 (ppm)
11. NO? (hot) read/3% 02 (ppm)
12. NO (cold) read/3% 02 (ppm)
13. Carbon Dioxide (%)
14. Carbon Monoxide (ppm) uncor/cor
15. Hydrocarbon (ppm) uncor/cor
16. Sulfur Dioxide (ppm) uncor/cor
17. Smoke Spot (Bacharach)
18. Atmos. Temp. (°F/°C)
19. Dew Point Temp. (°F/°C)
20. Atmos. Pressure (in. Hg)
21. Relative Humidity (%)
22.
23.
24.
25.
26.
27.
28.
29.
30.
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OPERATING DATA
Location 15
OHIT A
Test No.
Date
Time
Test Description
Oil Temp., »F
Fuel Press.
Eng. Oil Press. , pel
Water Temperature, °F
(Out of Heat Exchanger)
Steam Pressure, psi
Exhaust Temperature, "F
(Into Heat Exchanger)
Load, MW
Current, KA
Inlet Manifold Press.
Right/Left, in. H_0
Aftercooler Temp.
(water), *F
Inlet Manifold Temp.
Right/Left, °F .
Engine RPM
Load Unit B, MW/KA
Load Unit C, MW/KA
Load Onit D, MW/KA
Fuel Level (in.) /Tank So.
Fuel Consumption, gal/hr
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OPERATING DATA
Location 15
UHIT A
Test No.
Date
Time
Test Description
Oil Temp., »F
Fuel Press.
Eng. Oil Press., psi
Water Temperature, °F
(Out of Heat Exchanger)
Steam Pressure, psi
Exhaust Temperature, °F
(Into Heat Exchanger)
Load, MW
Current, KA
Inlet Manifold Press.
Right/Left, in. HO
Aftercooler Temp.
(water)j °F
Inlet Manifold Temp.
Right/Left, CF
Engine RPM
Load Unit B, MW/KA
Load Unit C, MW/KA
Load Unit D, MW/KA
Fuel Level (in.) /Tank No.
Fuel Consumption, gal/hr
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-------
OPERATING DATA
Location 15
UNIT A
Test No.
Date
Time
Test Description
Oil Temp.; "F
Fuel Press.
Eng. Oil Press., psi
Water Temperature, °F
(Out of Heat Exchanger)
Steam Pressure, psi
Exhaust Temperature, °F
(Into Heat Exchanger)
Load, MW
Current, KA
Inlet Manifold Press.
Right/Left, in. HO
Aftercooler Temp.
(water), *F
Inlet Manifold Temp.
Right/Left, °F .
Engine RPM
Load Unit B, MW/KA
Load Unit C, MW/KA
Load Unit D, MW/KA
Fuel Level (in.)Aank No.
Fuel Consumption, gal/hr
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OPERATING DATA
Location 15
OMIT A
Test No.
Date
Time • '
Test Description
Oil Temp., °P
Fuel Press.' •
Eng. Oil Press. , pai
Hater Temperature, *F
(Out of Heat Exchanger)
Steam Pressure, psi
Exhaust Temperature, *F
(Into Heat Exchanger)
Load, MH
Current, KA
Inlet Manifold Press.
Right/Left, in. HO
Af tercooler Temp . •
(water), °F
Inlet Manifold Temp.
Right/Left, •.?.-
Engine RPM
Load Unit B, HH/KA
Load Unit C; MH/KA
Load Unit D, MH/KA
Fuel Level (in.)/Tank No.
Fuel Consumption , gal/hr
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834
-------
OPERATING DATA
Location 15
UNIT A
Test Ho.
Date
Time
Test Description
Oil Temp., °F
Fuel Press.
Eng. Oil Press., psi
Water Temperature, °F
(Out of Heat Exchanger)
Steam Pressure, psi
Exhaust Temperature, °F
(Into Heat Exchanger)
Load, MW
Current, KA
Inlet Manifold Press.
Right/Left, in. HO
Aftercooler Temp.
(water) , °F
Inlet Manifold Temp.
Right/Left, °F .
Engine RPM
Load Unit B, MW/KA
Load Unit C, MW/KA
Load Unit D, MW/KA
Fuel Level (in.)/Tank No.
Fuel Consumption, gal/hr
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OPERATING DATA
Location 15
UNIT A
Test No.
Date . J .
time
Test Description
Oil Temp., °F
Fuel Press.
Eng. Oil Press., psi
Water Temperature, °F
(Out of Heat Exchanger)
Steam Pressure, psi
Exhaust Temperature, °F
(Into Heat Exchanger)
Load, MW
Current, KA
Inlet Manifold Press.
Right/Left, in. H_O
Aftercooler Temp.
(water), °F
Inlet Manifold Temp.
Right/Left, °F
Engine RPM
Load Unit B, MW/KA
Load Unit C, MW/KA
Load Unit D, MW/KA
Fuel Level (in.) /Tank No.
Fuel Consumption, gal/hr
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OPERATING DATA
Location 15
UNIT A
Test No.
Date
Time
Test Description
Oil Temp., °F
Fuel Press.
Eng. oil Press., psi
Water Temperature, °F
(Out of Heat Exchanger)
Steam Pressure, psi
Exhaust Temperature, ,°F
(Into Heat Exchanger)'
Load, MW
Current, KA
Inlet Manifold Press.
Right/Left, in. H.,0
Aftercooler Temp.
(water), °F
Inlet Manifold Temp.
Right/Left, CF
Engine RPM
Load Unit B, MW/KA
Load Unit C, MW/KA
Load Unit D, MW/KA
Fuel Level (in.) /Tank No.
Fuel Consumption, gal/hr
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OPERATING DATA
Location 15
UNIT A
Test No.
Date
Time
Test Description
Oil Temp. , °F '
Fuel Press.
Eng. Oil Press. , psi
Water Temperature, °F
(Out of Heat Exchanger)
Steam Pressure, psi
Exhaust Temperature, °F
(Into Heat Exchanger)
Load, MW
Current, KA
Inlet Manifold Press.
Right/Left, in. HJ3
Aftercooler Temp.
(water) , °F
Inlet Manifold Temp.
Right/Left, °F
Engine RPM
Load Unit B, MW/KA
Load Unit C, MW/KA
Load Unit D, MW/KA
Fuel Level (in.) /Tank No.
Fuel Consumption, gal/hr
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-------
OPERATING DATA
Location 15
UWIT A
Test No.
Date
Time
Test Description
Oil Temp. , °F
Fuel Press. *
Eng. Oil Press., psi
Water Temperature, °F
(Out of Heat Exchanger)
Steam Pressure, psi
Exhaust Temperature, °F
(Into Heat Exchanger)
Load, MH
Current, KA
Inlet Manifold Press.
Right/Left, in. HO
After cooler Temp.
(water) , °F
Inlet Manifold Temp.
Right/Left, CF .
Engine RPM
Load Unit B, MW/KA
Load Unit C, MW/KA
Load Unit D, MW/KA
Fuel Level (in. )/Tank No.
Fuel Consumption, gal/hr
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OPERATING DATA
Location 15
UNIT A
Test No.
Date
Time
Test Description
Oil Temp. , CF
Fuel Press.
Eng. Oil Press., psi
Water Temperature, °F
(Out of Heat Exchanger)
Steam Pressure, psi
Exhaust Temperature, °F
(Into Heat Exchanger)
Load, MW
Current, KA
Inlet Manifold Press.
Right/Left, in. HJ3
Aftercooler Temp.
(water) , °F
Inlet Manifold Temp.
Right/Left, °F .
Engine RPM
Load Unit B, MW/KA
Load Dnit C, MW/KA
Load Unit D, MW/KA
Fuel Level (in.) /Tank No.
Fuel Consumption, gal/hr
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OPERATING DATA
Location 15
UNIT A
Test No.
Date
Time'
Test Description
Oil Temp. , °F
Fuel Press.
Eng. Oil Press., psi
Water Temperature, °F
(Out of Heat Exchanger)
Steam Pressure, psi
Exhaust Temperature, °F
(Into Heat Exchanger)
Load, MW
Current, KA
Inlet Manifold Press.
Right/Left, in. HO ,
Aftercooler Temp.
(water) , "F
Inlet Manifold Temp.
Right/Left, °F .
Engine RPM
Load Unit B, MW/KA
Load Unit C, MW/KA
Load Unit D, MW/KA
Fuel Level (in.) /Tank No.
Fuel Consumption, gal/hr
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OPERATING DATA
Location 15
UNIT A
Test No.
Date
Time
Test Description
Oil Temp., °F
Fuel Press.
Eng. Oil Press. , psi
Water Temperature, °F
(Out of Heat Exchanger)
Steam Pressure, psi
Exhaust Temperature, °F
(Into Heat Exchanger)
Load, MW
Current, KA
Inlet Manifold Press.
Right/Left, in. H.O
Aftercooler Temp.
(water) , °F
Inlet Manifold Temp.
Right/Left, °F
Engine RPM
Load Unit B, MW/KA
Load Unit C, MW/KA
Load Unit D, MW/KA
Fuel Level (in.) /Tank No.
Fuel Consumption, gal/hr
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-------
LOCATION 15
Fuel Oil Analyses
Test 15-10 Test 15-11
4-19-77 , 4-21-77
1230 Hours , 1100 Hours
Carbon, % , 86.95 86.70
Hydrogen, % 12.79 12.65
t
Nitrogen, % ' . 0.008 0.008
Sulfur, % 0.28 0.24
Ash, % < 0.001 < 0.001.
Oxygen (by difference), % 0 0.40
API Gravity at 60 .°F 37.4 37.3
Gross Heat of Combustion, Btu/lb 19,520 19,400
Net Heat of Combustion, Btu/lb 18,350 18,250 ,
843
-------
Test NO.
tto-
PAKTICULATE EMISSION CALCULATIONS
Pate f-/.g-77 Location /J"" _
fuel
Enqr.
Sampling Train and Method JQX
Pitot Factor, Fs • 8 3
Barometric Pressure, P.
. «. ad Total
.^
S
«•>
in. Hg
gm
Tot. Uquid collected, V1
Velocity Head, AP -.f-f iwg Stack Temp., Ts__££7__eR Stack Area, As 0. 7»^ft2
Sample Volume, Vm &>* ft3 Stack Press., Psq ~.Z iwg Excess 02< «>a% }• ^ \
Orifice Press. Diff., H . t>£~ iwg Stack Gas Sp. Gravity, Gs /.OS n.d.
Sample Time, 6 9o min Nozzle Dia., Dn
•1. Sample Gas Volume Vm . . - 0.0334 Vm(P. + H/13.6)
in. Meter Temp., T
Vwstd - 0.0474
2. Water Vapor
3. Moisture Content Bwo • Bq. 2/(Bq. 1 + Eq. 2)
4. Concentration a. C • 0.0154 Mn/Vm
•td
3
•td
b. C - 2.205 x 10"6 Mn/Vm
c. C - Bq. 4b x 16.018 x 10
5. Abs. Stack Press. Ps • f^f x 13.6 •«•
6. Stack Gas Speed V* - 174 Fs
• Bq. 6 x As x
7. stack Gas Flow a.
Rate C 70°F
b. Qsd - Eq. 7a x (1. - Eq. 3)
8. Material Flow
9. XO, factor
10. Emission
11. % Isokihetic
Ms • Eq. 7b x Eq. 4b x 60
X02f • 2090/C20.9 - K32%)
«. E - Eq. 4b x Fe X Eq. 9
b. E - Bq. 4c x Fa x Bq. 9 x 1000
14077
6 x V» x P» x Dn
Fe SC Feet/104 Btu
Fn SC Meters/104 joules
Oil
92.2
0.002475
Gas
87.4
0. 002346
Coal
98.2
0.002636
0.
SCF
, SCF
N.D.
//ftg»/0 grains/DSCF
/ 76IX 'O lb/DSCF
grams/DSCM
in. w abs.
ft/min
HSCF/min
DSCF/min
Ib/hr
S3 9 3
• 3
Ib/MMBtU
ng/ j oule
•Multiply Vmgtd by 530/Tm(°R) if meter not temp, compensated.
Data Sheet 6002-4
844
-------
Test No.
Unit No.
PARTICULATE EMISSION CALCULATIONS
Date y-/3-?7 Location /-T
Fuel £ 0/4. Sampling Train and Method J*0/.
Engr.
Pitot Factor, Fs
Barometric Pressure, P 36>/9
_in. Hg
Tot. Liquid Collected, V /fl?..? ml Total Particulate, M J2& • V m gm
Velocity Head, AP
iwq Stack Temp., Ts_££2__eR Stack Area, As Q.7lf ft2
Sample Volume, Vm_j££__ft Stack Press., Psg -..£ iwg Excess 0 , XO % .
Orifice Press. Dif f . , H » ^ •»" iwg Stack Gas Sp. Gravity, Gs /,O3 n.d.
Sample Time, 8_£0_min v Nozzle Dia., Dn '/6 * % in. Meter Temp., T ^"3jC "R
*1. Sample Gas Volume Vm „. - 0.0334 Vm(P. + H/13.6)
sta bar
2. Water Vapor ^gtd " °'0474 vic
3. Moisture Content Bwo • Eq. 2/(Eq. 1 + Eq. 2)
etd
4. Concentration a. C • 0.0154 Mn/Vn
b. C - 2.205 x 10"6 Mn/Vin
c. C • Eq. 4b x 16.018 x 10
5. Aba. Stack Press. Ps
std
3
Pbar x 13.6 + Psg
6. Stack Gas Speed V» - 174 Ps /APTs /|22. x •ig
7. Stack Gas Flow a. Qew - Eq. 6 x As x x
Rate 0 70°P T8
ZS_
407
b. Qsd - Eq. 7a x (1. - Eq. 3)
8. Material Flow Me • Eq. 7b x Eq. 4b x 60
XOjf - 2090/(20.9 - X02%)
10. Emission a. E • Eq. 4b x Fe x Eq. 9
9. XO. factor
11. % Isokinetic
b. E » Eq. 4c x Fm x Eq. 9 x 1000
14077
9 x V» x Ps x Dn
F« SC Feet/104 Btu
Fm SC Meters/104 joules
Oil
92.2
0.002475
Gas
87.4
0.002346
Coal
98.2
0.002636
•Multiply Vm . . by 530/T (°R) if meter not temp, compensated.
SCO ID
'
SCF
SCF
N.D.
X
grains/DSCF
'lb/DSCF
grams/DSCM
in. w abs.
ft/min
WSCF/min
DSCF/min
Ib/hr
N.D.
Ib/MMBtu
ng/joule
Data Sheet 6002-4
84 5
-------
Test No.
ttait No.
PARTICULATE EMISSION CALCULATIONS
Date V-S3- 77 Location.
Fuel *
Engr.
Sampling Train and Method
Pitot Factor, Fs » S3
Tot. Liquid Collected, V.
Ic-
Barometric Pressure, P.^. SO-/^" in. Hg
ml Total Particulate, M_ m gm
Velocity Head, AP 0.
iwq Stack Temp.
Stack Area, As_
ft
Sample Volume, Vm
Stack Press., Psg -»
_iwg Excess 0,, JJO,%_
Orifice Press. Diff., H O.S& iwg Stack Gas Sp. Gravity, Gs n.d.
Sample Time, 9 «?;?.-*" min Nozzle Dia., Dn . W in. Meter Temp., T ,
•1. Sample Gas Volume Vm . . - 0.0334 Vm(P. + H/13.6)
std . bar
2. Water Vapor Vw - 0.0474 V
3. Moisture Content Bwo - Eq. 2/CEq. 1 + Eq. 2)
4. Concentration a. C • 0.0154 Mn/Vm
std
b. C - 2.205 x 10"6 Mn/Vm
C. C - Eq. 4b X 16.018 X 10
5. Abs. Stack Press. Ps - P * 13.6 + Psg
std
3
409.1
6. Stack Gas Speed Vs • 174 Fs VAPTs 1-^-
7. Stack Gas Flow a. Qsw - Eq. 6 x As x -— x -r^r
Rate 8 70°F 8 4O'
b. Qsd • Eq. 7a x (1. - Eq. 3)
8. Material Flow Ms • Eq. 7b x Eq. 4b x 60
K>2f - 2090/{20.9 - X02%)
10. Emission . a. E - Eq. 4b x Fe x Eq. 9
9. K>2 factor
11. % Isokinetic
b. E - Eq. 4c X Fm x Eq. 9 x 1000
14077 x Ts (Vm + Vw )
i — =r—
6 x Vs x Ps x Dn
/jr. /? see
SCF
r*o
N.D:
grains/DSCF
Ib/DSCF
grams/DSCM
in. w aba.
ft/min
HSCF/min
DSCF/min
Ib/hr
N.D.
Ib/MMBtu
ng/joule
Fe SC Feet/104 Btu
Fm SC Meters/104 joules
Oil
92.2
0.002475
Gas
87.4
0.002346
Coal
98.2
0.002636
•Multiply Vm8td by 530/Tm(°R) if meter not temp, compensated.
Data Sheet 6002-4
846
-------
Test No. 4T--if Date_
Unit No. ¥
PARTICULATE EMISSION CALCULATIONS
77 Location
Engr.
Sampling Train and Method joy
Pitot Factor, Fs » 83
f
Barometric Pressure, P. gtf/O/ jn. Hg
ml Total
Tot. Liquid Collected, V^ //?
Velocity Head, AP • 34" jwq Stack Temp., Ts
a gm
»R stack Area," As 0. 7SJ>'tt2
Sample Volume, Vm
ft
3
stack Press., Pag -.01 iwa Excess 0,, XO % Vtf.
Orifice Press. Diff., H_
Stack Gas Sp. Gravity, Gs //O3
n.d.
Sample Time, 9 /3.I min Nozzle Dia., Dn__££__in. Meter Temp., T*__£££__<1R
*1. Sample Gas Volume Vm . . - 0.0334 Vm(P. ' + H/13.6)
sta oar
2. Water Vapor Vw d - 0.0474 V.
3. Moisture Content Bwo • Eq. 2/(Eq. 1 + Eq. 2)
gtd
atd
3
4. Concentration a. C - 0.0154 MnAm
b. C - 2.205 x 10~6 Mn/Vm
c. C - Eq. 4b x 16.018 x 10
5. Abs. Stack Press. Ps • P]jar x 13.6 + Psg
6. Stack Gas Speed Vs - 174 Fs /APTs
7. Stack Gas Flow a. Qsw • Bq. 6 x As x - x f...
Rate 3 70eF Ts 407
b. Qsd - Eq. 7a x (1. - Eq. 3)
8. Material Flow
9. XO. factor
10. 'Emission
11. % Isokinetic
MB • Eq. 7b x Eq. 4b x 60
XO f - 2090/(20.9 - X02%)
a. E • Eq. 4b x Fe x Eq. 9 •
b. E - Eq. 4c x Fm X Eq. 9 x 1000
14077 x Ts(V»
I -
Btd
Vwatd)
6 x Vs x Ps x On
Fe SC Feet/104 Btu
Fm SC Meters/104 joules
Oil
92.2
0.002475
Gas
87.4
0.002346
Coal
98.2
0.002636
•Multiply Vta ... by 530/T (-R) if meter not tenp. coiqpensated.
•EQ w -
SCF
SCF
grains/DSCP
. 0*)
/* Ib/DSCF
grams/OSCM
in. w abs.
ft/min
WSCF/min
DSCF/min
Ib/hr
N.O.
Ib/MMBtu
ng/joule
Data .Sheet 6002-4
847
-------
PARTICULATE EMISSION CALCULATIONS
Test No. /.f- 9P Date f-/J"-?7 Location /jT
No. f Fuel *^?
.^_^B_
f 3
sampling Train and Method -3"OX .
_^HM^_^
Engr.
Pi tot Factor, Fs
Barometric Pressuret P. 30*g/
oar
in. Hg
Tot. Liquid Collected, V. // g ml Total Particulate, M_ /g?> / m gm
ic ~ ' * ' " ' n
Velocity Head, & . 3-i" iwg Stack Temp. , Ts y.5"6 "R Stack Area, Aa
Sample Volume, Va 62 ft3 Stack Press., Psg ~« ° > iwq Excess 0 , XO %
Orifice Press. Dif f . , H • /£ iwg Stack Gas Sp. Gravity, Gs />Q3
i^—.2
n.d.
Sample Time, 6 /£/ min "Nozzle Dia., Dn
in. Meter Temp., T -f-S9
*1. Sample Gas Volume Vm ,_ - 0.0334 Vm(P. + H/13.6)
sta oar
2. Water Vapor Vw - 0.0474 V
3. Moisture Content Bwo » Eq. 2/(Eq. 1 -I- Eq. 2)
4. Concentration a. C • 0.0154 Mn/Vm
-6
std
b. C - 2.205 x 10 Mn/Vm
c. C • Eq. 4b x 16.018 x 10
std
3
5. Abs. Stack Press. Ps - P. x 13.6 + Psg
6. Stack Gas Speed Vs - 174 Fs /APTs Jjj2- x ^
7. Stack Gas Flow a. Qsw - Eq. 6 x As x {-^ x |2
Rate 6 70eF 8 40
b. Qsd - Eq. 7a x (1. - Eq. 3)
00
8. Material Flow
9. K>2 factor
10. Emission
11. % Isokinetic
Ms - Eq. 7b x Eq. 4b x 60
XO f - 2090/(20.9 - XO %)
a. B - Eq. 4b x Fe x Eq. 9
b. E « Eq._ 4c-x Fm x Eq. 9 x 1000
14077 x Tfl (Vm + VW )
I - — f^~
9 x Vs x PS x Dn
Fe SC Feet/104 Btu
Fm SC Meters/104 joules
Oil
92.2
0.002475
Gas
87.4
0.002346
Coal
98.2
0.002636
909
//91
S/OO
• »¥
SCF
SCF
•9.
N.D.
grains/DSCF
Ib/DSCF
grams/DSCM
in. w abs.
ft/min
WSCF/min
DSCF/min
Ib/hr
N.D.
Ib/MMBtu
.ng/joule
•Multiply Vm by 530/T (°R) if meter not temp, compensated.
Data Sheet 6002-4
848
-------
PARTICULATE EMISSION CALCULATIONS
Test No. /Jj"-y.T Date ^-/J^-77 Location,
Unit No. Fuel ^g
Engr. 2%)
a. E • Eq. 4b x Fe x Eq, 9
b. E - Eq. 4c x Fm x Eq. 9 x 1000
14077
9 x Ve x Ps x Dn
Fe SC Feet/104 Btu
Fm SC Meters/104 joules
Oil
92.2
0.002475
Gas
87.4
0.002346
Coal
98.2
0.002636
•Multiply Vmstd by 530Am(*W i* meter not temp, compensated.
09
SCF
SCF
N.D.
grains/DSCF
Ib/DSCF
grams/OSCM
in. w abs.
ft/min
WSCF/min
DSCF/min
Ib/hr
N.D.
Ib/MMBtu
ng/joule
Data Sheet 6002-4
849
-------
Test No ._
Ottit No.
PARTICULATE EMISSION CALCULATIONS
Date 4f'/9-77 Location /f
Engr. K .
Fuel *jt
_Sampling Train and Method
Pitot Factor, Fs
Tot. Liquid Collected,
Barometric Pressure, t Jf9-t9 in. Hg
ml Total Particular, M S3L.7 m gm
Velocity Head, AP 0. 3O iwg Stack Temp. , Ts
*R Stack Area, As » 7?*"" ft
Sample Volume, Vm &2Z ft3 Stack Press., Psq
Orifice Press. Dif f . , H .
iwg Excess Q^, XO %
iwg Stack Gas Sp. Gravity, Gs
n.d.
Sample Time, 6 3 6 c min Nozzle Dia., Pn i/a in. Meter Temp., T
*1. Sample Gas Volume Vm M » 0.0334 Vb(Pbar -I- q/13.6)
2. water Vapor w td " O-0474 vlc
3. Moisture Content Bwo • Eq. 2/(Eq. 1 + Eq. 2)
. /
4. Concentration a. C - 0.0154 Mn/Vm
std
b. C • 2.205 x 10~6 Mn/Vm
c. C - Eq. 4b x 16.018 x 10
std
3
SCF
SCF
N.D.
grains/DSCF
Ib/DSCF
5. Abe. Stack Press. Ps • P. x 13.6 + Psg
6. Stack Gas Speed Vs - 174 Ps eVs x
1.00
Gs
/. 3YX'Q grams/DSCM
W'<* in. w abs.
3.3*0
407
7. Stack Gas Flow a. Qsw » Eq. 6 x As x
Rate 8 70»F TS
b. Qsd • Eq. 7a x (1. - Eq. 3)
MSCF/min
DSCF/min
8. Material Flow Ms • Eq. 7b x Eq. 4b x 60
X02f - 2090/(20.9 - X02%)
a. E • Eq. 4b x Fe x Eq. 9
b. E « Eq. 4o x Fm x Eq. 9 x 1000
11. % Isokinetic . 14077
9. XO factor
10. Emission
N.D.
i
Ib/MMBtu
ng/joule
8 x Vs x Ps x Dn
Fe SC Feet/104 Btu
Fm SC Meters/104 joules
Oil
92.2
0.002475
Gas
67.4
0.002346
Coal
98.2
0.002636
•Multiply Vm . by 530/T (•R) if meter not teiqp. conpenaated.
•ca •
Data Sheet 6002-4
^ y.y +(.**.)
850
-------
Test No.
unit No.
PARTICULATE EMISSION CALCULATIONS
Date ?-2/- 77 Location,
Fuel^?
Engr.
sampling Train, and Method
Barometric Pressure, P 30»
bair
Hg
ml Total Particulate, M, S3O min Nozzle Dia., Dn 0-jr in. Meter Temp., T "I
•1. Sample Gas Volume Vm . . - 0.0334 Vm(P. + H/13.6)
sta bar
2. Water Vapor Vw . . « 0.0474 V,
std ic
3. Moisture Content Bwo • Eq. 2/(Eq. 1 + Eq. 2)
39.7
SCF
SCF
4. Concentration a. C =• 0.0154 Mn/Vm .
std
b. C • 2.205 x lo"6 Mn/Vm
c. C =• Eq. 4b x 16.018 x 10
std
3
__._£££_ N.D.
Q. OOJT7 grains/DSCF
~ Ib/DSCF
5. Abs. Stack Press. Ps - P. x 13.6 + Psg
oar
6. Stack Gas Speed Vs « 174 Fs /APTs lj!± x •=£=
7. Stack Gas Flow a. Qsw » Eq. 6 x As x ——' x TT:=
"Rate 9 70°F
b. Qsd - Eq. 7a x (1. - Eq. 3).
8. Material Flow
9. X02 factor
10. Emission
11. % Isokinetic
Ms • Eq. 7b x Eq. 4b x 60
X02f - 2090/(20.9 - XD2%)
a. E • Eq. 4b x Fe x Eq. 9 .
b. E • Eq. 4c x Fffl x Eq. 9 x 1000
14077 x
I .
/. 8/ y/O~ grams/DSCM
_ in. w abs.
_ ft/min
._ WSCF/min
_ DSCF/min
y
_ Ib/hr
_N.D.
_ Ib/MMBtU
_ ng/joule
9 x Vs x Pa x Dn
Fe SC Feet/104 Btu
Fm SC Meters/104 joules
Oil
92.2
0.002475
Gas
87.4
0.002346
Coal
98.2
0.002636
•Multiply Vmat. by 530/T (°W if meter not temp, compensated.
Data Sheet 6002-4
- 8
85 1
-------
Test No.
Box No.
~-£- f
/
Test Description
PARTZCULATE CALCULATION SHEET
Date
-77 Location
Test Crew
Sample Probe Position
Dry Gas Meter Vol. (ft )
Final 33*6.33
Initial 3 ait . S3
Total &A.OO
Inpinger Water Vol (ml)
1 2
Final /?y //g
Initial /& o soo
A Vol W /*
Beaker No. .5- H 3
Date .
Weighed 'ft/ '7
Tare 1 9 y . 9 3 «^~
Wt. 2 *^
3
4
5
6
Avu 9«. 930 f
Bottle No. J+*
Impinger
Content (Water)
Rinse (ml) bJlf
Date Weighed
or 250 Bake y-^V-77
Final 1 99.0 /^i"
Wt. 250 2 ??. 0 /a- 3
3
4
5
6
Avg 99. o'ff
Residue wt ,of/9
Final 250-Tare
Date Weighed
or 650 Bake
Final 1
Wt. 650 2
3
4
5
6
Avg
Residue Wt
Final 650-Tace
fOO. &O£~<*
^
/
3
Probe
(Acetone)
ra-r
SOO. 6 /-ft
s
/ee. f»/ ft
. o/o *
jo/. 9S/X
^
/O/. 1S/J
y
Probe
(Water)
AOO
/o/. 9*0,1
/o/. 9tt^"
/e/,99t7
.OOff
Atno/uf
BL**)k.
y
/OO. 78 f£
^
/eo.ltft
Cyclone
(Acetone)
/OO
tOO.TVlO
Soo. it1) a.
/0o,?S9/
.00*3
3 S. Gel~ Total
3 £f3.o ?*>7.0
o tst.t ?39. 8
a. /3. a /oj.x
#ao
SLAAK.
1 /
/eo.07*3
• i^
/OO.0731
Flask
(Dry)
/OO
/«e. tltt
•
/S6.»ttl
,00**
Filter
No.
;?-*-
. 233?
.8339
, 8*39
, f 7*-f
•
. fi 7JTS"
.oy/6
Blank
No.
*(,
. ZV-Tf
. «yj-&
. S?-f~6
•
.S?f7
>/
.gff?
^
Comments i
Data Sheet 6002-3
852
-------
PARTICULATE CALCULATION SHEET
Test No._
Box No. ~
Test Description
Date 4f-/f-~?7 Location
Sample Probe Position
Test Crew
Dry Gas Meter Vol. (ft )
Impinger Water Vol (ml)
Final 3y33.OO
Initial 3340. oo
Total CS.oO
Beaker No. 7
Date
Weighed f-3-77
Tare 1 /j/. OQIA"
Wt. 2 <—
3
4
5
6
AW M.&OIS'
Bottle No.
Impinger
Content (Water)
Rinse (ml) ^ **"
Date Weighed y./8~?7
or 250 Bake
Final 1 tot. /jti,S
Wt. 250 2 •
3
4
5
6
AVB IOt
-------
>LAH-T
..OCATION
)PERATOR
METHOD 5 CONTROL CONSOLE READINGS
UJN NO.
iAMPLE BOX NO.
IETER BOX NO.
1ETER H
-FACTOR"!
AMDIENT TEMPERATURE
BAROMETRIC PRESSURE '
ASSUMED MOISTURE, % "
HEATER BOX SETTING "
PROBE LENGTH, IN.
NOZZLE DIAMETER, IN."
PROBE HEATER SETTING"
SCHEMATIC OF STACK CROSS SECTION
Traverse
Point
Nunber
-
-
. TOTAL
Sampling
Time
t~\ HJ —
^^^^^WWWT.
C.Jioe.iL
TS*J0 00
/o/y
/asif
Static
Pressure
<**>'
In. Mf.
^•.o
-.^
(#**>&•&
i
Stack
Tempera-
ture
{TS) «F
320
z> &LO,
#00
Voo
#00
Voo
0
Velocity
Head
.».>
. 4A'
^ ^ M
.^^
.6J."
.6^'
.L±"
.t*
Pressure
Differen-
tial Acros
Orifice
Meter
(AH),
In. H2O
.J-f
IZZJ.*?
.96
.$<.
.*(.
.8(,
.$<*
s Gas
Sample
Volume
(vm) ft3
3^/«.«
3*a>«.#o
TO &
339V. 00
333T-O
s
S~0
JTft.
J~a
s~/
^9
CO
en
-------
JLAHT__
-OCA.TION
OPERATOR
)ATE
METHOD S CONTROL CONSOLE READINGS
V-/3-7-7
tUN NO. __
SAMPLE BOX NO.
JETER BOX NO. *-//-/»»/
1ETER H '
: -FACTOR"! "
AMBIENT TEMPERATURE
BAROMETRIC PRESSURE "
ASSUMED MOISTURE, % "
HEATER BOX SETTING "
PROBE LENGTH, IN.
NOZZLE DIAMETER, IN."
PROBE HEATER SETTING"
JOL.
SCHEMATIC OF STACK CROSS SECTION
Traverse
Point
Nuiber
:
..
TOTAL
Sampling
Time
I— kX***^fc.
£4««,K.
Tj^nf
///o
11 9^
. H-&O
il32
Static
Pressure
.^J."
.(.*
.LIT
Pressure
Differen-
tial Acros
Orifice
Meter
(AH),
In. H2O
.B<,
.*(*
,U
a Gas
Sample
Volume
»p
go
?o
*s
AVG.
Sample
Box
remprta-
ture
OF
Avn
Temperature
of Gas
• Leaving
Condenser on
jast Impinger
°F
*r
^y
&*-
CO
en
-------
PLANT
LOG AT I OH _
OPERATOR Pj>
DATE ».A--7-7"
METHOD 5 CONTROL CONSOLE READINGS
RUN NO. AS-- 3
SAMPLE BOX NO.
METER BOX NO. "
1ETER H ~~
: FACTOR"?"
AMBIENT TEMPERATURE
BAROMETRIC PRESSURE "
ASSUMED MOISTURE, % '
HEATER BOX SETTING "
PROBE LENGTH, IN.
NOZZLE DIAMETER, IN."
PROBE HEATER SETTING"
so.or
l/y
SCHEMATIC OP STACK CROSS SECTION
Traverse
Point
Number
;
;
i
i
i
TOTAL
WCRAGH
Sampling
Time
^~ijj^^^
»»^«*W*»
Ci.CC.C-
TW»ir
A3~
o ^e>o
o9/-i"
0930
/O SA~
/oVL
Static
Pressure
(Ps),
In. Hi?.
H+O
-.0*
'
t
Stack
Tempera-
ture
(Ts) »P
3*0
3$*'
VoO
Voo
yoo
yoo
Velocity
Head
(P8)
.33.
.2^
.3f
.*<>'
.3*'
.3*
Pressure
)if feren-
tial Acres
Orifice
Meter
(AH),
In. H20
.
33-?£..oe>
33SV-00
3Vo(..oo
31/32, ao
Gas Sample
Temperature at
iry Gas Meter
Inlet
(Tmin.)
«P
Outlet
(Tmout>
°F
6*
t*'
7S
12
9*
9*'
AVG.
»vn.
Sample
Box
remprta-
ture
•P
300
3'*"
32.0
3/i>"
3**'
333'
' *
AVfi
Temperature
of Gas
Leaving
Condenser on
uast Impinger
•F
/ 3
-------
PLANT
LOCATION
OPERATOR
DATE
METHOD 5 CONTROL CONSOLE READINGS
t, -^--
RUN NO. xjs--g-
SAMPLE BOX NO.
DIETER BOX NO. '
4ETER H ~~
: -FACTOR"?
AMBIENT TEMPERATURE
BAROMETRIC PRESSURE "
ASSUMED MOISTURE, % "
HEATER BOX SETTING "
PROBE LENGTH, IN.
NOZZLE DIAMETER, IN."
PROBE HEATER SETTING"
SCHEMATIC OP STACK CROSS SECTION
CO
en
Traverse
Point
Nvaber
TOTAL
WERAGr
Sampling
Time
/^\j|^_»
f^OAt.
/too
///*>"
//3o
/'*/
Static
Pressure
3
Gas Sample
Temperature at
Dry Gas Meter
Inlet
(Tmin.)
•P
Outlet
(Tmout>
•P
fs
93
?€
11
AVG.
AVG.
Sample
Box
remprta-
ture
•P
AV(i-
Temperature
of Gas
Leaving
Condenser on
*ast lapinger
°P
60
<>*
C2-
L3
-------
ANDERSEN CASCADE IMPACTOR DATA
00
en
oo
Test No.
Impactor t
Stack Temj
Plate
1
2
3
4
5
6
7
8
Back Up
Filter
x:s-- £ .Z
Jo. /
jerature •?£ o
Tare (g)
J-7.3/SJ
\
j
i .
21. $8 o7 1
/7. *5-*3
J7.9(.I1
w»v
**-,*i*r '
»:»•*
Location
Nozzle Size
°F Inpac
Final (g)
27,3,r?
**. yy7/
*1.2<)>9
*/. 98-2?
,7. IS St.
n.9i*l
>7.<*7^
29.3 7-S'O
«/.7i,3
/-*
^^v/
tor Flow Rate
Net (g)
, <5<^<3 &
. 00*3
. OO 2 (+
,00 2.3
.00,*
.00/0
. 00 Jtf
. 0021
.00*
Owner
Filtei
%
^". 3.
:/
-------
ANDERSEN CASCADE IMPACTOR DATA
oo
en
-
ay. 7^07
Location
Nozzle Size
°F Impac
Final (g)
A*3/?.J
a.i.y^QS'
*9,j9x?
*,. 1S*o
n, 9f*/
/7.JL3/
1-7. 1731
2$ . 3807
a/.?«/o
/£>~~
Sif
tor Flow Rate
Net (g)
# ^ O / A*
• & & J2 ^>
.00 a )
.00*0
.
• No.
-TCFM
Cum. %
soo
<77,t
9/*o
?t>./
S/-3
7^.3
65. /
6AV
^.5 -
BCD (y)
„-/£.<}
*.l JO.V
*•? 7.0
V.o ?,S
3.C, 3. /
/. 3 /• 4
.» ,57
.fir .<*L
> r
/r
Data Sheet 6002-5
-------
PLUME OPACITY OBSERVATION RECORD
LOCATION MO.
OWNER ^
OBSERVER
DATE .4-13-77
_ BOILER NO.,
'FUEL TYPE
POINT OF EMISSION
Test Run No.
CAPACITY
BURNER TYPE
POINT OF OBSERVATION
4 7A 6. C. x/0 T
TO f £/fO
TEST
No.
/
*
3
y
S
L
7
s
9
/o
„
t*
13
11
!*'
I
Time
/*0f
•is"
••*
•If
/o tff
•If
30
«f
JO/1
A.'
to
vr
l*i*
„
Jo
If
Type
(*n
ltd iff
Test
Load
k#/hr
Opacity
3-
A"
/O
<,'
^
f
^'
.^-
<,'
O
j-
S
o
3
S
y
WIND
Speed
mph
-v-r
Direct
S*
Sky
Cond
U
*
et*.
*y
Sun
Posi-
tion
Comments
•
860
-------
PLUME OPACITY OBSERVATION RECORD
LOCATION NO.
OWNER '_
DATE
>-*
y -/j -77
POINT OF EMISSION
POINT OF OBSERVATION
Test Run No.
OBSERVER /H.0.M.
BOILER NO.,
FUEL TYPE
CAPACITY
klb/hr
BURNER TYPE
TEST
No.
n
19
11
40
a;
3*-
*3
*1
-
Tine
an/pm
/»/3
/A'
Jo
y^'
fOff
or
90
Vi'
Type
frf«r
>tui#re
Test
Load
k#/hr
Opacity
%
* ^-* s
Direct
£
U>
Sky
Cond
£4^/1*
a*y
Sun
Posi-
tion
-
Comments
86 1
-------
Project! •
Datai V-/3-77
Locations
Units '
VELOCITY TRAVERSE
TMt Description i
Stack Cross Section
*ssts_
Fuels
Hr»onn€l«
BaroMtrie Preis. (in. Bg)« 30-1.9
Absolute Static Press, in Stack (in.,
Pitot Tube Coefficients . 83
-. a.
-------
VELOCITY TRAVERSE
Tart Description!
Datat i
location!
Unltt.
Teatl
•tack CTOM S«cti6n
PwraonMl i
•trie Prats, (in. Bali 36. Q>
Absolute Static Praaa. in Stack (in. art i -.OS
Pitet Tuba Coafttctantt »?3
vs-B5-48S mr
11/2
TiM
Trav«r»* Point
Pott Depth
CW>*«
Velocity
Itead
(in. H,0)
AP
.33
Ga« Tu|>.
CP>
320
Gai tuaf.
<•»)
*8
Ji<0
Holacular
»t.
MS
Velocity
-------
Projecti
Date. ?-/ f - 7 7
locations
Dnitt
VELOCITY TRAVERSE
Test Description i__
Stack Cross Section
Test. X.T-X O
Personnel t
7. &
fuel. *J? 0/<-
.
Barometric Press, (in. Bg)i S9, 9 I
Absolute static Press, in Stack (in. WHi • 07
Pitot Tubs Coefficient!
- 85.48
.
TIM
Traverse Point
Port Depth
*T*t*.
^,"
Velocity
Bead
(in. H,0)
AP
. 3JT
Gas Tem>.
CF)
V/7
Gas Temp.
CR)
TS
S77
Molecular
wt.
»«s
Velocity
(ft/se«H
vs
Oj
Cone.
(« Dry)
6002-13
864
-------
Project! EPA
Date i y-2,
location!
Unitt
VELOCITY TRAVERSE
jgT J/tefTest Description!
- 77
/.r
Stack Cro«« Section
P«r«onn«l i
Testi_
Fueli
Barometric Press, (in. Hg) i 3&' I f
Absolute Static Press, in Stack (in. Hg)i_
Pitot Tube Coefficient! r O 3
(P.)
Vg • 65.48
Time
Traverse Point
Port Depth
MCK
r
Velocity
Bead
fin. H,0)
fip
,37fa()
Gas Temp.
(•r)
V^2-
Gas Teagi.
CR>
Ts
Molecular
Wt.
is
Velocity
(ft/sec)
vs
02
Cone.
(% Dry)
-
6001-13
89.5
-------
Date
K V B. INC.
Teat NO. /T-6-.S
TEST NO.
UNIT NO.
SOx DATA SHEET
_ FUEL *?g/t LOAD jpo MaThr
location
Box No.
Time
Temp . in Gas Meter
Press, in Gas Meter
Meter Reading
Baron. Press.
Percent Oxygen
N2 Purge Time
x-*
s»ys
£•/
6
O
3«. /O
/0.0
!3/C
"Z-*
S30f
J~/
0 .
/,e>o
36. so
S&.0
S3 3 3
„ (A - B) x N x P x (460 + T) x 24
Excess Oj /C'Q %
so2
A • Ml of lead perchlorate used for sample - 9. 7
B - Ml of lead perchlorate used for bland • **• / "
N - Normality of lead perchlorate titrant - • $/«•**
P - Dilution factor - /O
T • Average temp, in gas meter • _rv/
V • Volume of gas sample ft3 « /tffl
P » Barometric pressure - 30. fQ
p "Pressure in gas meter - O
Concentration. C, ppm • w »
.um/d.cm -
Emission - ,B» g/Mcal • j]
. * •" >'
B - Csf 2090 1 Ib/MsiS''-
^'s-xoaj
C • pollutant concentration, g/dscm
P, volume factor » __dscm/10 cai
..,.,.;„. dsef/104 Btu
from Fed. R«g. 9/11/74 p 32856
so3
7.6
I./
, e/of
/
*"'/
/,*-&
30.lt>
0
/ tl
(4 / T
60-14
rev.
"k
1
L/2/75
866
-------
Date
K V B. INC.
Test No.
~ 5
TEST NO.
UNIT NO.
SOx DATA SHEET
*
FUEL 2 O'L LOAD
Location
BOX NO.
Time
Temp, in Gas Meter
Press, in Gas Meter
Meter Reading
Barom. Press.
Percent Oxygen
N2 Purge Time
?'/
/jxy
-TV
o
o
2o. /o
/0'&
/3?V
•?-/
133*-
f~/
O
/.oo
30. 1C
/o.o
//o3
\.
Calculation: S03 or S02, ppm = (A " B) x N \* * j4^ ^ T) x 24
Excess 02 '°'°._ %
A = Ml of lead perchlorate used for sample =
B = Ml of lead perchlorate used for bland =
N = Normality of lead perchlorate titrant =
F - Dilution factor =
T B Average temp, in gas meter =
V - Volume of gas sample ft3 •=
P m Barometric pressure =
p - Pressure in gas meter =
Concentration^, ppm =
E "
2090 1
°-9-x02j
P, volume factor
from Fed. Reg. 9/11/74 p 32856
_dscm/10 cal
Btu
Emission-,E, g/Mcal "
Ib/MBtu •
where *• "J "9/J -
C • pollutant concentration, g/dscm
so2
7-8-
(..(
. 0/QS~
/o
-f-'S
S'OQ
3o. /o
o
73
so3
7,9 .
L.f
.O'0^~
t
^-//
/.t>0\
30- /O
0
7-7
^
I
i
1
1
1
1
60-14
rev. 1/2/75
867
-------
Date
K V B. INC.
Test No.
SOx DATA SHEET
TEST NO./-*"'6" UNIT NO.
*?tf/A LOAD 5»tf -&»"«
Location V.*'
Box No.
Time
Temp, in Gas Meter
Press', in Gas Meter
Meter Reading •
Barom. Press .
Percent Oxygen
N2 Purge Time
-x-z
)3.0
SfO*'
t-*-
/?£>&,
3~2-
O
/,6O
30-' &
SO. 0
/?3/
(A - B) x N x F x (460 + T) x 24
Excess o? /->>O %
.; .', S02
A » Ml of lead perchlorate used for sample = *?•%
B a M! of lead perchlorate used for bland = £•/
N » Normality of lead perchlorate titrant ™ . o/o£~
F a Dilution factor =• to
T » Average temp, in aas meter a -S"/V
V a Volume of gas sample f t3 a /. Of>
P a Barometric pressure a 3O./O
p a Pressure in gas meter a o
Concentration. C, ppm a s3 _
t gm/dscm ••
Emission -.E. g/Mcal •
E - CP[ 2090 1 Ih/MBtii "
B0.9-XO, I
where «• J ng/J
C • pollutant concentration, g/dscm
pr volume factor - .jdscm/10 cal
dscf/104 Btu
from Ped. Keg. 9/11/74 p 32856
so3
7-8T
6>.l
. oto±~
/
&/
Ad-0
30.'*
O
7.*-
60-14
rev. :
sox
L/2/75
868
-------
KVB. INC.
Test Mo. /T- 9-3.
TEST NO.
UNIT NO.
SOX DATA SHEET
FUEL ** ONLOAD
Location /•£•'
Box No.
Time
Temp, in Gas Meter
Press, .in Gas Meter
Meter Reading
Barom. Press.
Percent Oxygen
N2 Purge Time
-X.'*
/iS7
70
O
o
30,03"
/o./
/*/*
TL-/
/£//
7O
O
/.f>00
30. OS"
/o.t
/2ZSL-
•
Calculation: SO. or SO., ppm «
Excess 02 /O' / %
(A - B) x N x F x (460 + T) x 24
V {P + p)
A - Ml of lead perchlorate used for sample =
B a Ml of lead perchlorate used for bland •=
N s Normality of lead perchlorate titrant -
F * Dilution factor •>
T •* Average temp, in gas meter -
V * Volume of gas sample ft3 =
P <• Barometric pressure -
p * Pressure in gas meter «
Concentration^, ppa "
,gm/d«cin •
Emission-,E, g/Mcal •
Ib/KBtu "
ng/J -
C • pollutant concentration! g/dscn .
r, • volume factor - d«cm/10 oal
d«cf/10* »«-,
so2
<^.7
V.t
.o/oz
/o
^•30
/.BOO
3O.OST
O
9*
'
,• .
so3
6. ?
-------
Date V-A»— 77
K V B. INC.
Test No. AS"- 7,5
SOx DATA SHEET
TEST NO. AT-?5 UNIT NO.
FUEL
LOADVfrO
Location
Box No.
Time
Temp, in Gas Meter
Press, in Gas Meter
Meter Reading
Barom. Press .
Percent ^Oxygen
N2 Purge Time
t'*
tUt*
7/
0
o
30.0 if
/a./
/*33
%-Jt
t*3 a.
73
O
/,ooo ,
30.0^
/O.I
/30 0
'•.
,
• . i •
„,
Calculation: S03 or S02, ppm = (A- B) x N x^x ^460 + .T) x 2.4
Excess 02 /Q'l »
A = Ml of lead perchlorate used for sample =
B = Ml of lead perchlorate used' for bland -
N « Normality of lead perchlorate titrant =
F = Dilution factor =
T - Average temp, in gas meter =
V "Volume of gas sample ft3 =
P = Barometric pressure =
p m Pressure in gas meter =
Concentration,C, ppm =
,(jm/dscm •
Emission-,E, g/Hcal "
Ib/MBtu '
ng/J «
E -
where
of 2090 1
bo.a-xOj I
:a L J
so2
c,.-?
*(*
.oto*.
/O
JT32.
/,ooo
30.03-
0
92
;.-
so3
/*.o
*.£.
.6/03.
/
*33
/,e>oo
36-ox'
O
3S>.*-
sox
r
1
.
C • pollutant concentration, g/dscm
F, volume factor - __ dscm/10 cal
from Fed. Rag. 9/11/74 p 32856
Btu
60-14
rev. 1/2/75
870
-------
Date y-ur- 77
K V B, INC.
Telt NO.
TEST NO
./*"'4
UNIT NO.
SOx DATA SHEET
FUEL$*><- LOAD
Location •/S"
Box No.
Time
Temp, in Gas Meter
Press, in Gas Meter
Meter Reading
Barom. Press.
Percent Oxygen
N2 Purge Time
-x.-'
/a/A
73
O
0
3 0.0 A"
/*~
/O.I*
. /3<*£
•
460 + T x 24
Excaae Oj /6 • 1 %
SO,
A • Ml of lead perchlorate used for sample - £•£
B » Ml of lead perchlorate used for bland » V- 4
N » Normality of lead perchlorate titrant • <6/6d.
F - Dilution factor - /<9
T • Average temp, in gas meter • -T33
V • Volume of gas sample ft? - ^/ £ £0
P » Barometric pressure • ^o.o^
p « Pressure in gas meter • 0
Concentration »C. ppm • So
.«m/d.an -
Emii«ion-.E. g/Mcal «
B - CFJ" 2090 Ib/MBtii •
wh«r« L J ng/J - .
C - pollutant concentration, g/dscn .
p, ««!««• factor - , dacm/10 cal
d.cf/104 B1.u
from Fed. Beg. 9/11/74 p 32856
S03
£.?
V-d»
.o/o»
/
.T33
/ooo
3aojr
0
?.6
60-14
rev.
sox -
1/2/75
87 1
-------
LOCATION 15
Fuel Tank Capacity Chart
Inches
1
2
3
4
5
6
7
8
9
10
11
12
13
14
15
16
17
18
. 19
20
21
22
23
24
25
26
27
28
29
30
31
32
33
34
35
36
37
38
39
40
41
42
Gallons
9
25
46
70
98
128
160
195
232
271
311
353
397
• , 442
488
535
584
633
685
735
788
841
895
950
1006
1062
1119
1176
1235
1292
1351
' 1410
1470
1529
1590
1650
1710
1771
1832
1893
1954
2015
Inches
43
44
45
46
47
48
49
50
51
52
53
54
55
56
57
58
59
60
61
62
63
64
65
66
67
68
69
70
71
72
73
74
75
76
11_
78
79
. 80
81
82
,33
84
Gallons
2076
2138
2198
2259
2320
2380
2441
2501
2561
2620
2679
2738
2795
2854
2912
2968
3025
3080
3135
3189
3242
3295
3346
3397
3447
3495
3543
3589
3634
3677
3719
3760
3798
3835
___ -3BM
3902
3933
3960
3985
4005
^402L
4030
872
-------
TABLE TRACE SPECIES AND ORGANICS
SAMPLING CONDITIONS - LOCATION 15 DIESEL ENGINE
TS&O Run No.
Test No.
Date
Port Location
Velocity, m/s (f/s)
Stack Temp., K (°F)
Oxygen Content, % dry
Moisture, %
Sample time, min.
Cyclone Flow, awcmm (awcfm)
Isokinetic Rate, %
Oven Temp., K (°F)
XAD-2 Temp., K (°F)
Meter Temp., K (°F)
Nozzle Size, mm (in. )
No. Filters Used
Sample Flow, Dry, scmm (scfm)
Volume Collected, Dry, scm (scf)
Particulate weight, g
Solid Participates, ng/J (Ib/MMBtu)
1
15-10
4/19/77
Q, (6")
11.9 (39)
485 (414)
10.1
5.6
300
0.103 (3.64)
114
479 (403)
291 (64)
298 (77)
12.7 (0.5)
1
0.059 (2.08)
17.55 (624.1)
0.2367
6.43 (0.0149)
2
15-11
4/21/77
q, (6")
12.8 (42)
486 (415)
10.3
5.9
300
0.105 (3.72)
108
482 (408)
290 (61)
302 (83)
12.7 (0.5)
1
0.060 (2.12)
18.00 (635.8)
0.2364
6.39 (0.0149)
873
-------
KVB
SASS SAMPLING CONDITIONS
Test Site Location '
Sample Port Location
Stack Conditions: Stack Velocity 33V& ft/min T 60 « V <= .O ft/sec
~™ •""•-™^— "-"••"• ^-^— _• •••-• «™ -•—•——•-•
Stack Temp. X-5 °F + 460 = T = g 7-3 " °R
S -- Lunn _. - - -
Stack Moisture; BWQ = g . 3£ %
Particulate Loading (Method 5) , C » o. o SL<» grams/DSm
Probe Nozzle Size for 4.0 ACFM (wet) through cyclones at 400 °F:
Isokinetic Size = 0.1192 x /T /V «= 0 ,-S-g-iT inches
s s -
Closest Actual Nozzle Size, D «= £> '-£~& inches
n —————
% Isokinetic @ 4 WACFM, Actual Nozzle = 1.421 x T /(V xD2) «=
s s n
If % Iso not in range of 90 to 110%, Adjust Cyclone Flow by:
Q • 2.814 x (% Iso) x V x D2/T = 3. M? wet ACFM
xcyc s n' s -
If % Iso @ 4 WACFM is greater than 110, use (% Iso) = 110
If % Iso @ 4 WACFM is less than 90, use (% Iso) =90 :
Orifice Pressure Differential, H -
Meter Temp. , T = <£ " in. H.O
m o m - 2
Dry Gas Volume to be Collected (5 hour run)
V =:Q_ x 60 x 5 = jT 73 ,9 DCF
m nn -
Estimated Condensate Collection •— ; ----
V. = V x 530 X B / [0.0474 x T x (1. - B )] - t>~9> f.J ml
Ic m wo m wo -
Estimated Particulate Collection
M «= C x V x 530/(T x 35.3) •= O• V * grams
n o m .
Dafca
-------
KVB
SASS SAMPLING CONDITIONS
Test Site Location / «?
Sample Port Location
Stack Conditions: Stack Velocity 2-?c'/c> ft/min T 60 = V = 3j, * ft/sec.
" S ""* ,
Stack Temp. V/5" °F + 460 = T = g"75" °R
" S ^MB
Stack Moisture; B = x 0700 (&s f.
Particulate Loading (Method 5), C = 0,0J2 /" grams/DSm
Probe Nozzle Size for 4.0 ACFM (wet) through cyclones at 400 °F:
Closest Actual Nozzle Size, D = 0, 5~ inches
n - ! —
% Isokinetic @ 4 WACFM, Actual Nozzle = 1.421 x 1 / (V xD2) = /2 £. 5" %
s s n - -
If % Iso not in .range of 90 to 110%, Adjust Cyclone Flow by:
Q = 2.814 X (% ISO) XV x D2/T = J^/^7 wet ACFM
eye s n s - ' -
If % Iso @ 4 WACFM is greater than 110, use (% Iso) = 110
If % Iso @ 4 WACFM is less than 90, use (% Iso) = 90
Orifice Pressure Differential, H
- . ,,
Meter Temp. , T, = ff5" °F + 460 = 5'Y$' °R (use 560 °R for estimate)
m - - -
Meter Flow Rate, Q = Q x T x (1. - B )/860 = 2- '& 3 DCFM
xm eye m wo - —
Orifice No. (1, 2, 3) = _2 _ , 3 = 0.78, D = 0.281 , J x D2 = 0.062
Orifice Press Diff . , H <= 1.108 x (Q /J D2)2/! = j?"<2 / in. H_O
m o m - . . 2 •
Dry Gas Volume to be Collected (5 hour run)
V =0x60x5= DCF
m Tn - -
Estimated Condensate Collection
V, = V x 530 x B / [0.0474 x T x (1. - B )] = _ ml
Ic m wo m. wo - -
Estimated Particulate Collection
M = C x V x 530/(T x 35.3) = _ grams
n m m ' - •
875
Data Sheet 6002-17
-------
Projecti £PA
HI
KVB, INC, TRACE SPECIES AND ORGAN ics SAMPLING DATA
r/os****
Personnel i Jfag.eJt.Ty Barometric Press > St9- 9
Dates
Location:
Units
Tests
Fuels
4-/1-7 7
/^r
y
/j--xo
•* & QS4-
4e>o
/**>
3/0
J?VO
300
Traverse
Point
Depth
*>*
£
6
£
£
6
£
6
£
6
Pitot
OP
(in H2O)
>3f
.30
.30
.£0
.30
.30
.30
.30
x 30
.SO
Orifice
AP
(in H20)
3.W
J>.0f
J.OJT
jt.osr
a.oir
H>6f
Ji.ojT
j.ojr
J.OJT
a.of
CUB.
Meter
Volume
(ft3)
6/a,3on
6W.ou>o
yot.oeoo
7ti.oooo
g3i.«ooo
fcs.Voajt
taj.loaz
oy&.7ooQ
/?/. 0000
^3V.30I7
Pump
Suction
(in. Hg)
t,*r
"?
£(*
At
Inpinger
Out
•s-y
&s
t?
63
60
\**»T
ij"
Ljr
to
A3
Oven
320
40*
VO?
#eS
?OJT
401
407
VOL
407
Hater
in/Out
»v>
7/
90
sy
SI
Zl
S7
97
9o
4*.
63
6JT
7¥
79
V
79
20
£0
°2
Cone.
% dry
CO
-sj
o>
-------
Project: EPA PHASf M
KVB, INC, TRACE SPECIES AND ORGANics SAMPLING DATA
Personnel! P/Wf5SA Barometric Press t 30.
Dates V-%2/- 77
Locations /5~
Unitt
Tests /5~-//
Fueli ** 2- &l L.
fe>0 tf^ f4Sft.S/(J£
Probe Nozzle Diameter (inches) i
Absolute Static Press, in Stack
Pitot Tube Coefficients
. //
(in. Kg). -. 4fS
.93
(Dn)
(PS)
(CP)
T I
Real
0725-
Og?5~
012?
elS?
103.5-
/eSf
toff
IIT6
I2&
I3&
\ E
Elapsed
O
30
£0
10
1 20
IF0
Ifff
310
2-70
$00
. --_ _
Traverse
Point
Depth
<*
("
•c«
f"
£"
e"
("
s"
£"
Pitot
AP
(in H2O)
.30
.35-
.3?
.3?
.3$-
.)s-
.35-
.3?
.35-
.
Orifice
AP
(in H20)
j.*J~
3.2
2.3-
-
2.2.
2-2.
c/f4/V
2.2
2.2.
2.2.
2.2.
Cun.
Meter
Volume
(ft3)
2&.6000
2,1 f. 1000
3ti.qo#>
<(S7.#>00
ffOWl
££0
f&.yiuf
f 77.0000
W.WO
9(1.1X2
_ _- -_
Pump
Suction
(in. Hg)
5:f
£.2.
£.?
7.2
j.3
PS£5/<
V.?
i
tfeS"
t*7
V/2.
f*(
Ht*
_.
Meter
In/but
7i
86
gg
12.
f^
10
12.
10
12.
&
71
7f
&>
?l
91
22
72.
Z3
o2.
Cone.
% dry
. . . __
GO
-------
TRACE SPECIES AND ORGANICS TEST
SAMPLE RECOVERY LOG
Test No. IS-tO Date 4 - >ft-77 Location 15
Sample Port Position S~TAC.V£ -
•.—8 7 8
-------
Teat No.
TRACE SPECIES AND ORGANICS VEST
SAMPLE RECOVERY LOG
Date 4—-1&-TT Location 15 "!£)IB*.
Sanple Port Position
Container
Number
Sample Description
Container
Type
Net
wt/vol.
Comment
E 54-1
100%
ISO*
M 1042.
G»viHT S-
L-5
Data Sheet KVB 6002-15
879
-------
DIESEL ENGINE
TEST 15-10
TABLE STACK
POLLUTANT
SAMPLE NUMBER
Antimony
Arsenic
Barium
Beryllium
Cadmium
Calcium
Chromium
Cobalt
Copper
Iron
Lead
Manganese
Mercury
Nickel
Selenium
Tellurium
Tin
Titanium
Vanadium
Zinc
Chloride
Fluoride
Nitrates
Sulfates
563*
to
a
•3
541
3Z-
2.0
/3oo
IU
^2.00
02.00
<5
* du~
41
ipito
60
/ooo
3(0
2.0
0-15
•Z..O
o./o
3.3
tfo.OOS
o.Sl
0.050
"oTX'r
o.lfo
0.02.0
0.030
2..0
O./O
0-08
O.Sfc
O.01O
-------
DIESEL ENGINE
TEST 15-10
TABLE
STACK
POLLUTANT
SAMPLE NUMBER
Antimony
Arsenic
Barium
Beryl Hum
Cadmiiim
Calcium
Chromium
Cobalt
Copper.
Iron
Lead
Manganese
Mercury
Nickel
Selenium
Tellurium
Tin
Titanium
Vanadium
Zinc
Chloride
Fluoride
Nitrates
Sulfates
dugtt
cat
3.S
4.3
3.5
in
0.87
-------
DIESEL ENGINE
TEST 15-10 TABLE WAOC
POLLUTANT SAMPLE NUMBER ^
Antimony
Arsenic
Barium
Beryllium
Cadmium
Calcium
CluroinxuD
Cobalt
Copper
Iron
Lead
Manganese
Mercury
Nickel
Selenium
Tellurium
Tin
.<'
Titanium
Vanadium
Zinc
Chloride
Fluoride
Nitrates
Sulfates
706*
T-
^0.2.
<:o.ot.
oJV
5
O.OI
-------
COMMERCIAL TESTING & ENGINEERING CO.
QENEHAL OFFICE!: «»0 NOHTH LA OAILE OT»EET, CHICAGO, ILIINOIO 00601 • AHEA CODE 113 790-0414
Reply tO INSTIUMENTAl ANALYSIS DIVISION. 14139 WCST 44TH AViNUI. COIDIN. COtOIAOO 00491, PHONE: 301-27t-9S>l
To: Mr. John C. Mlchalovlc V*ifciK
Calspan Corporation ^Hff"^
Post Office Box 235
Buffalo, NY 14221 .
\
P. 0. No.:
Sample No.: Test 15-10 Al
Date: July 6, 1977
Analyst: S. Sweeney
IAD No.: 97-A345-1 34-21
CONCENTRATION IN pg/ml
ELEMENT CONC.
Uranium ^).2
Thorium <).2
Bismuth
Lead 0.7
Thallium
Mercury NR
Gold <0.02
Platinum '
Irldlum
Osmium
Rhenium
Tungsten
Tantalum
Hafnium
Lutetlum
Ytterbium
Thulium
Erbium
Hoi ml urn
Dysprosium
ELEMENT CONC.
Terbium
Gadolinium
Europium
Samarium
Neodyml urn
Praseodymium 0.02
Cerium 0.04
Lanthanum 0.07
Barium 0.8
Cesium 0.03
Iodine 0.04
Tellurium
Antimony 0.04
Tin
Indium STO
Cadmium
Silver 3
Palladium
Rhodium
ELEMENT
Ruthenium
Molybdenum
Niobium
Zirconium
Yttrium
Strontium
Rubidium
Bromi ne
Selenium
Arsenic
Germanium
Gallium
Z1nc
Copper
Nickel
Cobalt
Iron
Manganese
Chromium
CONC.
0.7
0.1
0.9
0.007
0.07
0.08
0.03
<0.01
0.5
0.3
0.7
0.03
5
0.04
0.2
ELEMENT
Vanadium
Titanium
Scandl urn
Calcium
Potassium
Chlorine
Sulfur
Phosphorus
Silicon
Aluminum
Magnesium
Sodium
Fluorine .
Oxygen
Nitrogen
Carbon
Boron
Beryllium
Lithium
Hydrogen
CONC.
0.3
0.2
10.01
MC
5
1
MC
MC
3
0.4
5
MC
=1
NR
NR
NR
0.04
<0.001
NR
NR - Not Reported
All element* not reported <0.02pg/ml
Approved:
883
-------
COMMERCIAL TESTING & ENGINEERING CO.
OCNCIMI. OrrtClt: lit HOtTH LA »ALLI »T«IT, CMIOAOO, ILUHOI* 10*01 • AltA CODC l» 781-1414
Reply to iNsratiMCNTAi ANALYSIS DIVISION, tan WIST MTH AVINUI. OOIMM, COHMADO *MOI, PHONI, JOJ-JTMSII
To: Mr. John C. Mlchalovlc
Calspan Corporation
Post Office Box 235
Buffalo, NY 14221
Date: July 1, 1977
Analyst: S. Sweeney
P.O. No.: 27810
Sample No, Te$t .^
ELEMENT CONC.
Uranium 11
Thorium 2
Bismuth 0.4
Lead 200
Thallium
Mercury NR
Gold
Platinum
Ir1d1um
Osmium
Rhenium
Tungsten 6
Tantalum
Hafnium
Lutetlum
Ytterbium
Thulium
Erbium
Hoi ml urn
Dysprosium
CONCENTRATION IN PPM WEIGHT
V
ELEMENT
Terbium
Gadolinium
Europium
Samarium
Neodymlum
Praseodymium
Cerium
Lanthanum
Barium
Cesium
Iodine
Tellurium •-
Antimony
Tin
Indium
Cadmium
Silver
Palladium
Rhodium
CONC.
0.3
0.2
1
1
150
0.2
2
0.5
13
STD
1
24
ELEMENT
Ruthenium
Molybdenum
Niobium
Zirconium
Yttrium
Strontium
Rubidium
Bromine
Selenium
Arsenic
Germanium
Gallium
Z1nc
Copper
Nickel
Cobalt
Iron
Manganese
Chromium
IAD No.:
CONC.
16
0.3
20
1
300
1
5
2
6
<0.1
1
MC
130
47
21
270
14
64
97-A345-134-21
ELEMENT
Vanadium
T1 tanl urn
Scandium
Calcium
Potassium
Chlorine
Sulfur
Phosphorus
Silicon
Aluminum
Magnesium
Sodium
Fluorine
Oxygen
Nitrogen
Carbon
Boron
Beryllium
Lithium
Hydrogen
CONC.
27
41
<0.2
MC
MC
180
870
MC
MC
>140
MC
:>360
MC
NR
NR '
NR
880
<0.1
0.5
NR
NR - Not Reported
All elements not reported <0.1 ppm weight
Approved:
884
-------
COMMERCIAL TESTING & ENGINEERING CO.
GENUAL OFFICE*! t»» NORTH LA IALLE IT*C(T, CHICABO, ILLINOIt (0(01 • AREA COOC »1» 7a*-l4l4
Reply tO INSTIUMINTAl ANALYSIS DIVISION, I«JJS WIST 44TH AVINUI. GOIMN. COLOtAOO «040I, PHONE, M3-37I4S31
To: Mr. John C. Mlchalovlc ^
Calspan Corporation ^j
Post Office Box 235
Buffalo, NY 14221
P.O. No.: 27810
Sample No.: Test 15-10 F
1041 5/27
Date: July 1, 1977
Analyst: S. Sweeney
IAD No.:
97-A345- 134-21
CONCENTRATION IN PPM WEIGHT
1
ELEMENT CONC.
Uranium
J^^-*?-*
330
=5
NR
NR ,
NR
0.5
0.1
NR
quartt cruel b
885
-------
COMMERCIAL TESTING & ENGINEERING CO.
GENERAL OFFICE!: t» NORTH LA 1ALLC STREET, CHICAGO, ILLINOII tO«OI • A«IA COOI «tl 7««-«4§4
Reply tO INSTMIMINTAl ANALYSIS DIVISION. 1433S WBI 44TH AVINUI. GOlDfN. COlOtAOO MMOI, FHONCi JOJ-J7MSH
To: Mr. John 6. M1chalov1c
Calspan Corporation
Post Office Box 235
Buffalo, NY 14221
P.O. No.: 27810
Sample No.: Test 15.10 G Comp. of 898 + B 700, 699, 936,
B/27/777' 69°* 938 CONCENTRATION IN *"9/ral
Oat* July 5, 1977
Analyst: s. Sweeney
IAD No.: 97-A345-134-21
ELEMENT CONC.
Uranium 0.04
Thorium <0.03
Bismuth
Lead *0.2
Thallium '
Mercury NR
Gold
Platinum
Irldlum
Osmium
Rhenium
Tungsten
Tantalum
Hafnium
Lute t1 urn
Ytterbium
Thulium
Erbium
Holmlum
Dysprosium
*Heterogeneous
NR - Not Reported
All element* not reported
ELEMENT
Terbium
Gadolinium
Europium
Samarium
Neodymlum
Praseodymium
Cerium
Lanthanum
Barium
Cesium
Iodine
Tellurium
Antimony
Tin
Indium
Cadmium
Silver
Palladium
Rhodium
<0.003 ug/ml
CONC.
0.004
0.01
0.01
0.006
0.007
0.04
0.03
0.005
0.007
0.009
£0.008
STD
0.006
MC
ELEMENT
Ruthenium
Molybdenum
Niobium
Zirconium
Yttrium
Strontium
Rubidium
Bromine
Selenium
Arsenic
Germanium
Gallium
Z1nc
Copper
Nickel
Cobalt
Iron
Manganese
Chromium
Approved: " f
CONC.
0.2
0.004
0.02
0.003
0.2
0.001
£0.007
<0.01
0.03
<0.002
0.004
0.5
0.09
0.2
0.01
7
0.04
0.3
W*
ELEMENT
Vanadium
Titanium
Scandium
Calcium
Potassium
Chlorine
Sulfur
Phosphorus
Silicon
Aluminum
Magnesium
Sodium
Fluorine
Oxygen
Nitrogen
Carbon
Boron
Beryllium
Lithium
Hydrogen
^ '
CONC.
0.02
0.5
<0.004
. MC
9
0.2
MC
MC
0.4
>4
MC
MC
=•0.2
NR
NR
NR
0.002
<0.001
0.01
NR
^
886
-------
R.ply to
COMMERCIAL TESTING & ENGINEERING CO.
•CNCMk OFPIOMl It* NOITN LA 1AUI »T(IIT, OHIOAIO, lUINOtt 10191 • A*IA 0001 til Tl«.*4t4
IMTIUMINTM ANMVM DIVISION, I4*H WOT 44TN AVINUl OOiOM, COUMAOO KMOI, PMOHIi WOM91
A
Te> Mr. John G. M1chalov1c ^\
Calspan Corporation ^""l
Post Office Box 235
Buffalo. NY 14221
P.O. No., 27810
s.mpl. NO., Test 15-10 H 1042 LF Diesel Fuel
CONCENTRATION
ELEMENT CONC
Uranium Q.06
Thorium Q.05
Bismuth
Lead Q.06
Thallium
i
Mercury NR
Gold .
-------
TRACE SPECIES AND ORGANXCS TEST
SAMPLE RECOVERY LOG
Test No. 1S-U Date 4-/al/~n Location \S 1)>gg.gL
/
Sample Port Position S*TACVC
Container
Number
Sanple Description
Container
Type
Comment
AA
PKllOu
S42.
940
U "P
A
*<
vuu.t
560
0)1 1
Pier.
IOD-1
M-l
IC44-
(54-e.
•424-240
II kl
**y
*
Id
loS
IC*A
Uk
4O.O.I
54.4
\UP *
JHP_
S
i£_
S-£
L-a
LF-I
Data Sheet KVB 6002-15
888
-------
DIESEL ENGINE
TEST 15-11
TABLE STACK
POLLUTANT
SAMPLE NUMBER
Antimony
Arsenic
Barium
Beryllium
Cadmium
Calcium
Chromium
Cobalt
Copper
Iron
Lead
Manganese
Mercury
Nickel
Selenium
Tellurium
Tin
Titanium
Vanadium
Zinc
Chloride
Fluoride
Nitrates
Sulfates
542
5
0*1
-------
KVB Analysis Data
Sample Number POM's PCB's
298 < 1 ug/g < 1 ug/g
534 < 1 ug/g < 1 ug/g
534 (duplicate) < 1 ug/g < 1 ug/g
13-18 740 90 ug/g < 1 ug/g
13-18 282 49 ug/g < 1 ug/g
13-18 530 3.2 ug/g < 1 ug/g
13-18 1038 6.3 ug/g < 1 ug/g
13-18 1032 396 ug/g < 1 ug/g
13-18 1033 1 ug/g < 1 ug/g
13-18 1034 8 ug/g . < 1 ug/g
13-18 1034 (duplicate) 9 ug/g < 1 ug/g
13-24 735 513 ug/g < 1 ug/g
531 6.9 ug/g < 1 ug/g
1039 20 ug/g < 1 ug/g
1035 144 ug/g < 1 ug/g
1036 , 10 ug/g < 1 ug/g
1037 7.1 ug/g < 1 ug/g
1037 (duplicate) 8.5 ug/g < 1 ug/g
14 556 70.5 ug/g < 1 ug/g
568 104 ug/g < 1 ug/g
532 10.7 ug/g « 1 ug/g
532 (duplicate) 8.2 ug/g < 1 ug/g
15-10 1041 <0.1 ug/g <1 ug/g
1041 (duplicate) < 0.1 ug/g < 1 ug/g
. 1042 * *
15-11 941 < 1 ug/1 < 1 ug/1
1044 < 0.1 ug/g < 1 ug/g
1045 * , *
19-1 LF * *
19-^2 533 < 0.1 ug/g < 1 ug/g
533 (duplicate) <0.1 ug/g <1 ug/g
C <1 ug/1 < 1 ug/1
C (duplicate) < 1 ug/1 < 1 ug/1
LF * *
*Sample extracts too concentrated to be able to determine an analytical value.,
890
-------
STEEL BILLET REHEAT FURNACE
Location No. 1>Unit No. \
Unit Description StEeTL.'BluL.erf,
Installation Date
Heater Rating S>5
Burner Description Mote.
U\^ (iHxMC^B^AvrN
.-ru AMOI? K.AK.N '11 2- 11
13-DU^uX^-L. UTopriR,^^t«T.^4fe^-^l4-^ ^TT^S^lOtf^
Test Fuel Combinations
Ki ^T « CaA<=.
Fuel Temp, at Burner (°F) A.»-^'C>\'S.V^T'
Primary Air Temp. (°F)
^MP,ii-ki-r
Comments:
89 1
-------
Test No._
Unit No.
MOBILE LABORATORY DATA
Date $~/J/77 Location
Fuel fiJrf-T. £45 Capacity
Test No.
Engr. U/JC
,/r
Unit Type /(? '#£//£ 47 f(J*AJjC£ Burner Type
~ 77
1. Test No.
2. Date
3. Time
4. Load
5. Process Rate. #/£*-£ ^////Z
6. Flue Diam. or Size/ -ft- ^t^.
7. Probe Position , -*V<^, ^^v
8. Oxygen (%)
9. NOx (hot) read/3% 02 (ppm)
10. NO (hot) read/3% 02 (ppm)
11. NO? (hot) read/3% 02 (ppm)
12. NO (cold) read/3% 02 (ppm)
13. Carbon Dioxide (%)
14. Carbon Monoxide (ppm) uncor/cor
15. Hydrocarbon (ppm) uncor/cor
16. Sulfur Dioxide (ppm) uncor/cor
17. Smoke Spot (Bacharach)
18. Atmos. Temp. (°F/°C)
19. Dew Point Temp. (°F/°C)
20. Atmos. Pressure (in. Hg)
21. Relative Humidity (%)
22.
23.
24.
25.
26.
27.
28.
29.
30.
////'/
f-7'77
/0y?-
£#
$~%
21 ^
/t.
2{
f1
2-f>
#
0
!• II-
/
77
70
73
2
7/
gf
5~S
X///-V
5-'J~77
/••irs
/5~>
2?
23
21
/2
0
6
Z3
77
gt>
t/£>
O
~7V
£1
jTf
/t//-5~
? -3-7 7
2'
^^
-^"
^
/$-,-?
23 72
22- 7?
2i ?2-
f 27
0 0
75-
fy
ff
, i
892
Data Sheet 6002-2
-------
Test No._
Unit No.
Date
MOBILE LABORATORY DATA
-/77 Location
Test No.
Engr.
Capacity
Unit Type/^ V .^
fc//!fiJ/tC£. Burner Type
1. Test No.
2. Date
3 . Time
4. Load
5. Process Rate./f///^/^//^
6. Flue Diam. or Size, ft
7. Probe Position
8. Oxygen (%)
9. NOx (hot) read/3% 03 (ppm)
10. NO (hot) read/3% 02 (ppm)
11. NO? (hot) read/3% 02 (ppm)
12. .NO (cold) read/3% O2 (ppm)
13. Carbon Dioxide (%)
14. Carbon Monoxide (ppm) uncor/cor
15. Hydrocarbon (ppm) uncor/cor
16. Sulfur Dioxide (ppm) uncor/cor
17. Smoke Spot (Bacharach)
18. Atmos. Temp. (°F/°C)
19. Dew Point Temp. (°F/°C)
20. Atmos. Pressure (in. Hg)
21. Relative Humidity (%)
22.
23.
24.
25.
26.
27.
28.
29.
JO.
/S//-*
^Y-77
0*ys~
$-?*&».
2-1^,
Sf-
/?
/^
2-0
y
^
f
£S
£2-
f*f
//
0
*5~
5~1
20, of
70
/£//- 7
5~-f-77
0ffe.
•7S
/^>
2-o
/B
/f
f
&
9
^?£f
G /
S2.
Sf
2-e
o
70
62^
?-*
5~'f-77
/0'-00
^ S
f @
/**'
2-t
/f
2-1
@
0
f
7£>
£3
70
2-7
&
^F ^5*
C^ &
f0
?0 r
-------
Test No..
Unit No.
MOBILE LABORATORY DATA
Date 5~-3'77 Location
Test No.
Engr.
Fuel
G,
Capacity
Unit Type l&
"
Burner Type X/,/?
1. Test No.
2. Date
3. Time
4. Load
5. Process Rate
6. Flue Diam. or Size, ft
7. Probe Position
8. Oxygen (%)
9. NOx (hot) read/3% ©2 (ppm)
10. NO (hot) read/3% 0^ (ppm)
11. NO? (hot) read/3% 02 (ppm)
12. NO (cold) read/3% O2 (ppm)
13. Carbon Dioxide (%)
14. Carbon Monoxide (ppm) uncor/cor
15. Hydrocarbon (ppm) uncor/cor
16. Sulfur Dioxide (ppm) uncor/cor
17. Smoke Spot (Bacharach)
18. Almas. Temp. (°F/°C)
19. Dew Point Temp. (°F/°C)
20. Atmos. Pressure (in. Hg)
21. Relative Humidity (%)
22.
23.
24.
25.
26.
27.
28.
29.
30.
////-//
F'1'77
2!?0 f
rz"
3-1
/?.
27
2-6
2-7
If
0
.0
*l
r$
fl
/%
2-Wr
*•
.. * e-
'
i
•
1
894
Data Sheet 6002-2
-------
Test No.
Unit No.
Unit
MOBILE LABORATORY DATA
Date 5~-5~-77 Location
Test No.
Engr.
g/f 5 Capacity,
Burner Type_
1. Test No.
2. Date
3. Time
4. Load
5. Process Rate "?*•*•* **,/#&
6. Flue Diam. or Size, ft
7. Probe Position
8. Oxygen (%)
9. NOx (hot) read/3% 02 (ppm)
10. NO (hot) read/3% 02 (ppm)
11. NO? (hot) read/3% 02 (ppm)
12. NO (cold) read/3% 02 (ppm)
13. Carbon Dioxide (%)
14. Carbon Monoxide (ppm) uncor/cor
15. Hydrocarbon (ppm) uncor/cor
16. Sulfur Dioxide (ppm) uncor/cor
17. Smoke Spot (Bacharach)
18. Atmos. Temp. (°F/eC)
19. Dew Point Temp. (°F/8C)
20. Atmos. Pressure (in. Hg)
21. Relative Humidity (%)
22.
23.
24.
25.
26.
27.
28.
29.
30.
/£//-&
$~~r-77
#336
5~ 2"
2?"
13.
2S
23
3
2(
/Y
&
o
-Tf
$~2
7
i7
33-
0
65-
5~t
2- % 7?
70
If//- 12-
r-r-77
/* yjr
/z
3^
j? ^?
^* ff
3.
2-f
/V
£>
/
4?
ft
1
£S
£2.
0
£7
5~*f
2 9- ?S
#3-
•
X//-/2-
/ J *
3-1
2-7
2-
2?
/i
o
I
£f
£3-
1
6f
32-
0
f£
£#
£4. IS
70
/f/l-^13-
5~-r-77
1230
/?r
/*/<
?>
3e
?/
3r
#
• 2.
^2
/f
#2-
13
O
70
So
2*?< f T
T*
////VJ
X-F
I'eo p
i^
: -•^*l
W*0
?i $7
33. y.r
,
$2 ¥2.
,
30 77^
& ' &
'
£*?.
-------
Test No._
Unit No.
Date
MOBILE LABORATORY DATA
~ 7 7 Location
Test No._
Engr.
Fuel
Capacity_
Unit Type
ffft/?4r
Burner Type
1. Test No.
2. Date
3. Time
4. Load
5. Process Rate
6. Flue Diam. or Size, ft
7. Probe Position
8. Oxygen (%)
9. NOx (hot) read/ 3% 0s (ppm)
10. NO (hot) read/3% 03 (ppm)
11. NO? (hot) read/3% 02 (ppm)
12. NO (cold) read/3% 02 (ppm)
13. Carbon Dioxide (%)
14. Carbon Monoxide (ppm) uncor/cor
15. Hydrocarbon (ppm) uncor/cor
16. Sulfur Dioxide (ppm) uncor/cor
17. Smoke Spot (Bacharach)
18. Atmos. Temp. (°F/°C)
19. Dew Point Temp. (°F/°C)
20. Atmos. Pressure (in. Hg)
21. Relative Humidity (%)
Tl.&'JtVf/ZZ OUT of 5£/£l//c£
23.
24.
25.
26.
27.
28.
29.
30.
///A/f
5~-6~-77
!32-
2.
'75/4,
5~?"
<2?
/?..
2-7
2?
3-7
fp
-------
Test No. J£f /
Unit No.
Pate
MOBILE LABORATORY DATA
Location _
Test No._
Engr.
Fuel
Capacity
Unit Type
#ftt£ft
C£ Burner Type
~t 7
1. Test No.
2. Date
3. Time
4. Load
5. Process Rate, j?/£.t-£T5'/kr
6. Flue Diam. or Size, ft
7. Probe Position
8. Oxygen (%)
9. NOx (hot) read/3% 03 (ppm)
10. NO (hot) read/3% 02 (ppm)
11. NO? (hot) read/3% 02 (ppm)
12. NO (cold) read/3% 02 (ppm)
13. Carbon Dioxide (%)
14. Carbon Monoxide (ppm) uncor/cor
15. Hydrocarbon (ppm) uncor/cor
16. Sulfur Dioxide (ppm) uncor/cor
17. Smoke Spot (Bacharach)
18. Atmos. Temp. (°F/°C)
19. Dew Point Temp. (°F/°C)
20. Atmos. Pressure (in. Hg)
21. Relative Humidity (%)
22.
23.
24.
25.
26.
27.
28.
29.
30.
H/J-/8
F-e-77
Ifi>e04
ft*
33
3t
32-
5£
0
3
/1
$3
ft
?7
£5~
5~£
21.11
5~~t
5~~S- 7 7
//t
5~J2-
...
897
Data Sheet 6002-2
-------
OPERATING DATA
• Location 16
. Unit 1
10 inch Reheat Furnace
Teat No.
X///--2
///A
/{//-$-
ate
f-3
Time
Soak Zone , •?
Z-/00
3-S00
Top Zone, °P
Soak Zone Air Flow, CFH
1 1.2-00
Soak Zone -Gaa Flow. CFH
Air Fuel Ratio Setpoint
Beating Zone Air Flow, CFH
70 000
fgoeo
Beating Zone Gas Flow, CFH
31000
Air Fuel Ratio Setpoint
Furnace Press. Setpt. , in. H,0
+.073
Fuel Flow Integrator
1770*0
BOOS
fvr tr
Load (billets per hour)
Billet Counter
-------
OPERATING DATA
Location 16
. Unit 1
10 inch Reheat Furnace
Test No.
Date
Time
//••PC
Soak zone, °F
2.12-2-
Top Zone, °F
/toe
Soak Zone Air Flow, CFH
'Soak Zone Gas Flow, CFH
Air Fuel Ratio Setpoint
Heating Zone Air Flow, CFH
Heating Zone Gas Flow, CFH
Air Fuel Ratio Setpoint
/t
tf
tf
Furnace Press. Setpt. , in. H,0
i-,073
Fuel Flow Integrator
177VH
1 77 ft *
BOOS
Load (billets per hour)
Billet Counter
899
-------
OPERATING DATA
Location 16
Unit 1
10 inch Reheat Furnace
Test No.
Date
Tine
Soak Zone, *F
Top Zone, °F '
Soak Zone Air Flow, CPH
Soak Zone Gas Flow, CFB
Air Fuel Ratio Setpoint
Beating Zone Air Flow, CFH
Beating Zone Gaa Flow, CFH
Air Fuel Ratio Setpoint
Furnace Press. Setpt. , in. B,O
Fuel Flow Integrator
BOOS
Load (billets per hour)
Billet Counter
I6/I-U
5--1
H • 70
2/Y0
/f20
WY00
9600
0
£5-000
ttfoe
+ (/
*-,073
47gfvr
/st>#£
900
-------
OPERATING DATA
Location 16
Unit 1
10 inch Reheat Furnace
Test No.
H//-I2-
16/t-t*.
/£//-/*•
K//-/3.
Date
r-f
ir-r-77
Time
Soak Zone, *F
Top Zone, *F
Soak Zone Air Flow, CFH
Soak Zone Gas Flow, CFH
/ffO.00
Air Fuel Ratio Setpoint
7-e
Beating Zone Air Flow, CFH
/0J000
Heating Zone Gas Flow, CFH
$£000
7*000
7^*00
Air Fuel Ratio Setpoint
- 1
Furnace Press. Setpt., in. IUO
+,0*
+.02
Fuel Flow Integrator
ft*/*!!
3-
BOOS
Load (billets per hour)
Billet Counter
r/sr
9 0
-------
OPERATING DATA
Location 16
Unit 1
10 inch Reheat Furnace
Test No.
////-/r /
-------
OPERATING DATA
Location 16
Unit 1
10 inch Reheat Furnace
Test No.
Date
Tine
Soak zone, *F
Top Zone, °F
Soak Zone Air Flow, CFH
Soak Zone Gas Flow, CFH
Air Fuel Ratio Setpoint
Beating Zone Air Flow, CFH
Heating Zone Gas Flow, CFH
Air Fuel Ratio Setpoint
Furnace Press. Setpt. , in. HJD
Fuel Flow Integrator '
BOOS
Load (billets per hour)
Billet Counter JVK/fif f Jri
////-//
10000
£~000
-r
1 eye oe
&/S00
f-/o
+-07
1W-OC
£>
«f2-
tf//-/$
r-f
//'05~
2*/5~
J.0#0
t3fe>o
?90e
-5~
/0t/eoe>
fS~000
/•//
+•-0*
?9Jf*t
e>
fir
K/t-rr
S-'<
/^ ->0f
2*/r
3.0 fo
/f?eo
/3. ?et>
-f
/etfooe
#7000
/-/-?
+*0*
-------
LOCATION 16
Fuel Gas Analysis
"2
CO <
Ethane '
Propane
Iso Butane
N Butane
Pentane
Pentane +
Organic sulfur
H2S
Heating Value
Specific Gravity
0.02% by volume
0.38%
1.27
93.36.
3-77
0.92
0.08
0.13
0.102
0.102
0.2 gr/100 SCF
0.01 grain/100 SCF
1049 Btu/SCF
0.5957
904
-------
. . GASEOUS FUEL ANALYSIS- -
Test
Unit
Fuel
Gas
CH4
C_H6
C3HB
C4Hin
C n
C5H12
24
C3H6
C4H0
C H
C,H
C0HC
N_
CO-
CO
H-
NO////
No. /£>" KM
Sample Point
Methane
Ethane
Propane
Butane
Pentane
Ethylene
Propylene
Butylene
Pentylene
Acetylene
Benzene
Oxygen
Nitrogen
Carb. Diox
Carb. Monox
Hydrogen
Date f
Fuel^
Test No
~'(~ 77 Location //"
Engr ,
8**<*M Btu CF fuel * / CF fuel *
WSCF Prod
10*> Btu
% Moisture
DSCF Prod
106 Btu
CF Prod
WSCF Prod (100 - % Moisture)
10«Btu
100
SCF air/10 Btu 9 70°F,
29.92 in. Hg.
Net SCF Prod/106 Btu
Dry SCF/10 Btu
% C02, dry
331.5x10
MH x (DSCF/106 Btu)
K' -K/430
lb/106 Btu - (ppm 9 3* 02)/K
ng/J - (ppm 9 3% OZ)/K'
K for
lb/106 Btu
K1 for
ng/J
Data Sheet 6002-6 (Rev. 1)
905
-------
PARTIOJLATE EMISSION CALCULATIONS
Test No. It// '19 Date 3 ~f ~ 77 Location //* Engr.
Unit No. / Fuel/#T ^V// Sampling Train and Method ,//*V7 -^5"
Pi tot Factor, 'Fs ' 03 Barometric Pressure, P. ^J.^G in. Hg
Tot. Liquid Collected, V l3f,5~ ml Total Parti culate, M ff-3 m gm
Velocity Head. &0-/3Z iwg Stack Temp., Ta/J/J~ "R Stack Area, As /<£
3 ft2
Sample Volume;
ft
stack Press., Psg "/..? iwg Excess 0,, TO % A?. /" ' %
Orifice Press. Dif f . , H
-------
PARTICULATE CALCULATION SHEET
Test No._
Box No.
Date r-f-r?
Test Crew
Location
I
Sample Probe Position
-fo//jr
Test Description
•Dry Gas Meter Vol. (ft )
Final ?^11.Oel2.
Initial JfSZ.Sfr
Total ft. 13 7
Impinger Hater Vol (ml)
1 2 3 S. Gel Total
Final 113 /J-/ 3 67J.i IIS'.H
Initial /off loo o ffff.f gio.q
AVol If */ 3 13.- f 13 f. r
Beaker No. f 4 ~7 %
Date
Weighed -T-J- 77
Tare 1 IX.f/lf
Wt. 2 —
3
4
5
6
AW 19.1/16
Bottle No. /
Impinger
Content (Water)
Rinse (ml) 77$~
Date Weighed
or 250 Bake 5~-/° ~77
Final 1 1 1. 13 3 S~
Wt. 250 2 —.
3
4
5
6
Avg 0. t*3l
2-
Probe
(Acetone)
fro
/ffO, V130
—
IOC. if 3 <*
,0e>1
-------
PLANT
LOCATION
OPERATOR"
DATE /
METHOD 5 CONTROL
READINGS
-f- 77
RUN NO. /6//-/S
SAMPLE BOX NO. /
METER BOX NO. /
4ETER H
: FACTOR"?"
.'93
AMBIENT TEMPERATURE
BAROMETRIC PRESSURE "
ASSUMED MOISTURE, % "
HEATER BOX SETTING "
PROBE LENGTH, IN.
NOZZLE DIAMETER, IN."
PROBE HEATER SETTING"
72-
SCHEMATIC OP STACK CROSS SECTION
1
Traverse
Point
Nuaber
TOTAL
WCRAGE
Sampling
Time
(a)Min.
£locK
rtrf£
looo
foty-
/0?0
t°ir
f/00
lt/5~
US*
iriT
12 O0
Static
Pressure
(Ps),
In. -Vg-HjO
-1.5
\
f
•
Stack
Tempera-
ture
(Ts) «F
^/2-
710
?te
?1I2-
W
#7?
$ZZ~
0
./o
,11
,10
.10
./f
,12-
.1$
.2.
.2-
?ressure
Differen-
tial Acres
Orifice
Meter
(AH),
In. H20
.is
.1~3
• It
.11
.?3
.?£
,70
,79
.$?
a Gas
Sample
Volume
Hf r» RSWIH6
Outlet
(Tmout>
•P
^
72.
#0
*t
12-
18
tea.
f*r
110
AVG.
ftUR
Sample
Box
remprta-
ture
•P
3J2.G
3io
2
&vr,
Temperature
of Gas
Leaving
Condenser on
^ast Impinger
•P
r?
fe>
5-0
?0
rz.
rr
rr
*0
?7
CD
O
oo
-------
PLUME OPACITY OBSERVATION RECORD
LOCATION NO.
OWNER
DATE
POINT OF EMISSION
POINT OF OBSERVATION
OBSERVER
BOILER NO.
VFUEL TYPE
Test Run No
. l6/f~
CAPACITY
Jclb/hz
BURNER TYPE
S 7~/t C ft
TO
TEST
No.
Time
am/pm
Type
Test
Load
k#/hr
L
Opacity
%
• .
WIND
Speed
. nph
Direct
Sky
Cond,
Sun
Posi-
tion
•
Comments !
1
i
i
i
•
i
i
i
909
-------
Projecti_
Datai
Locations
VELOCITY TRAVERSE
• T««t D«»criptioni
Cnitt
..• ' J. .. .
Testi
Stack Cross Section
Personneli
Barometric Press. ,(in. Hg):
Absolute Static Press, in Stack (in. Hg)._
Pitqt Tube Coefficient:
<
« 85.48
1/2
Tine
Traverse Point
Port ' Depth
:
•**,.
/0
>0
,S0f~
0
,<7
.etr
.2(9
Gas Ten>.
CF)
rfy
ffe>
i
ftr
1?5-
tST
y^o
1*0
llf
l?r.
70*
Gas Temp.
CR)
Ts
Molecular
Wt.
MS
Velocity
(ft/sec)
VS
Oj
Cone.
(% Dry)
•
6002-13
9 1 0
-------
»*ojacti_
Data I
Locationi_
Oniti _
VELOCITY TRAVERSE
Taet Daacriptioni
•tack Crof• Saction
Paraonnalt
Fueli
Bazooatrie Praia, (in. Bo)i 3 f.
Abaolvt* Static Pr«*t. in Stack (la. B«) i_
Pitot Tuba Coaffieianti
Vg - 85.48
V.
TiM
Travaria Point
Port Dapth
<***.
fo
20
Jo
to
re
5~6
r<
S~0
to
30
20
IO
Valoeity
Bead
(in. H,0)
AP
.37
.2-}
.1
,ovr
.63F
.0?
.ogf
.6>1
>*f
Mir
0AtfPt
Gaa Tup.
(•r)
7*0
?*0
ffo
Sea.
goo
goo
foe
f06>
22-0
(Sf>S£t
'XT IfOV
Gaa Taap.
CR)
Ts
'fiJG
Nolaettlaz
wt.
M8
Valoeity
(ft/aacf'.
vs
Oj
Cona.
(» Dry)
I
6001-11
91 1
-------
Date
K V B. INC.
Test No.
TEST NO./fcA'-^UNIT
SOx DATA SHEET
NO.
FUEL A/. 6. LOADSgMgjfjgb/hr Location
Box No.
Time
Temp, in Gas Meter
Press, in Gas Meter
Meter Reading
Barom. Press.
Percent Oxygen
N2 Purge Time
**-/
bios
lS°f=
•e-
-9-
3ft.fi/
/i"T8
o^fe
**-/
o^;y
S^lc
3-
l.o
10,0 /
)*-.B
07JT7
*-JL
otii
8J°F
-9-
-0-
10.01
is: a
O5?a
x-a.
09±-3
S-VP
-9-
l-O
3o.ol
/S-.B
/1-T.L! Tr^p .
Calculation:
Excess 02
SO. or SO., ppm
- B) x N x F x (460 + T) x 24
V (P + p)
A = Ml of lead perchlorate used for sample =
B = Ml of lead perchlorate used for bland «=
N = Normality of lead perchlorate titrant =
F = Dilution factor «
T = Average temp, in gas meter ('£.) =
V « Volume of gas sample ft3 e
P - Barometric pressure =
p = Pressure in gas meter =
Concentration,C, ppm =
,gm/dscm "
Emission-,E, g/Mcal •
Ib/HBtii "
ng/J -
E -
where
2090 |
o.a-xOj I
J
C - pollutant concentration, g/dscm
P, volume factor - dscm/10 cal
_dscf/lo4 Btu
from Fed. Reg. 9/11/74 p 32856
so2
T,7
: 5;^
^'O/^"
/
-------
Date
K V B. INC.
Test
l- 68
SOx DATA SHEET
TEST NO./b//-63 UNIT HO. foP-H FUEL M6>. LOAD'30#>/» kib/hr
Location
Box NO.
Time
Temp, in Gas Meter
Press, in Gas Meter
Meter Reading
Barom. Press.
Percent Oxygen
N2 Purge Time
-
" B) x N *
Calculations S03 or S<>2, ppm
Excess O2 • _ %
A = Ml of lead perchlorate used for sample =
B = Ml of lead perchlorate used for bland -
N.= Normality of lead perchlorate titrant -
F = Dilution factor =
T = Average temp, in gas meter «
V ** Volume of gas sample ft3 -
P = Barometric pressure =
p = Pressure in gas meter • «•
Concentration, C, ppm =
\
CFj 2090
C0.9-X
r, L
E - CFl 2090
where
Emission - ,E, g/Hcal •
Ib/MBtu '
ng/J -
C ° pollutant concentration, g/dscm
F, volume factor - dscm/10 cal-
from Fed. Reg. 9/11/74 p 32856
Btu
T) x 24
so2
^,7
<-.o
0.6/of
10
fit
1.0
3°, oi
31-1
so3
r./
s-.d
o.oi as"
1
S-V3
1.0
0,1
^x
i
ID.*
' .
\
60-14
rev. 1/2/75
9 1 3
-------
STEEL INGOT SOAKING PIT
Location No
. '<0 . Unit No. 7
Unit Description ^TEEU \Ki
-------
Test Mo..
Obit MO.
MOBILE LABORATORY DATA
pate 5~~~ /' 77 Location IS'
Fuel JJJT, G45 Capacity
Test No.
Engr.
Unit Type 504K/filG
Burner Type fi/0.
1. Test No.
2. Date
3. Time
4. Load
5. Process Rate
6. Flue Diam. or Size, ft
7. Probe Position
8. Oxygen (%)
9. NOx (hot) read/3% 02 (ppm)
10. NO (hot) read/3% 02 (ppm)
11. NO^ (hot) read/3% 02 (ppm)
12. NO (cold) read/3% O2 (ppm)
13. Carbon Dioxide (%)
14. Carbon Monoxide (ppm) uncor/cor
15. Hydrocarbon (ppm) uncor/cor
16. Sulfur Dioxide (ppm) uncor/cor
17. Smoke Spot (Bacharach)
18. Atmos. Temp. (°F/°C)
19. Dew Point Temp. (°F/°C)
20. Atmos. Pressure (in. Hg)
21. Relative Humidity (%) farf/A>)
22.
23.
24.
25.
26.
27.
28.
29.
30.
///2-/
f'0
,
»^
^_
*"^
i 7-/
7/ 72
70 y/
73 /t>2
7 *?
f* rg
o
-------
Test No._
unit NO.
Date
MOBILE LABORATORY DATA
Location
Test No.
Engr. W/f C
Fuel
Capacity
Unit Type
/ 7
Burner Type M0,
1. Test No.
2. Date
3. Time
4*. Load
5. Process Rate
6. Flue Diam. or Size, ft
7. Probe Position
8. Oxygen (%)
9. NOx (hot) read/3% 02 (ppm)
10. NO (hot) read/3% 02 (ppm)
11. NO? (hot) read/3% 02 (ppm)
12. NO (cold) read/3% 02 (ppm)
13. Carbon Dioxide (%)
14. Carbon Monoxide (ppm) uncor/cor
15. Hydrocarbon (ppm) uncor/cor
16. Sulfur Dioxide (ppm) uncor/cor
17. Smoke Spot (Bacharach)
18. Atmos. Temp. (°F/°C)
19. Dew Point Temp. (°F/°C)
20. Atmos. Pressure (in. Hg)
21. Relative Humidity (%)
22.
23.
24.
25.
26.
27.
28.
29.
30
K/2-6
5~~/0~77
0$ 00
~J J\ ~)
£*r
ff
H3
1*-
if
-?
/r
0
2
11
ft
5~2-
f
f
0
65~
5~1
30, to
7?
lf/J--7
5~'/0 -??
013S~
&f
VZ
ft
yi
•
#
&~
^
^«>«
y
f$~
?3
$-(
^
6
0
s£
60
3s, 1 0
7f
K/2--Z
F-/0-77
/0j#
£.
?JL
50
5*?
X
5~
&
-2.
S?
(1
61
/o
6
0
££
60
10,1$
7 (
/£/*--?
JTV/-77
0Z35'
f.
1?
tf
?0
0
Y
f~>
If
?y
/o
^^
&
&3-
5-7
30.03.
71
W/2-/0
5r-/!'77
Of/f
»^
^
-T,J
yy ?0
a &
n ?*
/0 If
^a J23
0 0
£2-
?7
30.02
9 1 6
Data Sheet 6002-2
-------
Test No._
Unit No.
MOBILE LABORATORY DATA
Date 5~~~// " 77 Location
Fuel /v G Capacity
Test
Engr.
Unit Type
Burner Type /t/4.
1. Test No.
2. Date
3. Time
4. Load
5. Process Rate
6. Flue Diam. or Size, ft
7. Probe Position
8. Oxygen (%)
9. NOx (hot) read/3% 0_2 (ppm)
10. NO (hot) read/3% 02 (ppm)
11. NO? (hot) read/3% 02 (ppm)
12. NO (cold) read/3% 02 (ppm)
13. Carbon Dioxide (%)
14. Carbon Monoxide (ppm) uncor/cor
15. Hydrocarbon (ppm) uncor/cor
16. Sulfur Dioxide (ppm) uncor/cor
17. Smoke Spot (Bacharach)
18. Atmos. Temp. (°F/°C)
19. Dew Point Temp. (°F/°C)
20. Atmos. Pressure (in. Hg)
21. Relative Humidity (%)
22.
23.
24.
25.
26.
27.
28.
29.
30.
/f/2-//
^~-//- 7 7
013$-
Ff7~
<±.
7.*
3$
37
vy
fz
3
s^y
/-2
^•r
o
tS/2-M
*'//' 77
///r
/,
$ro
V?
rs
/3-
3-0
O
f
??
5~&
5J
/3
2t
0
Ss
"^
"Ni
a
^
K
^
yT^
V>
/6/£-/~
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Data Sheet 6002-2
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Test No._
Unit No.
Date
MOBILE LABORATORY DATA
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Test No.
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Data Sheet 6002-2
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OPERATING DATA '
Location 16
Unit 2
Soaking Pit
Test No.
Date
Time
Pit Temp., °F
North Pit Temp., °F
Burner Position Control
Pit Pressure, in. H.,6
Battery Gas Press., psig
Flue Press.i in. H,0
Gas Flow Indie.. CFH x 300
Air Flow Indie., CFH x 3000
Fuel/Air Ratio Control
Total Gas Flow Indie.
(Two Pits)
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OPERATING DATA
Location 16
Unit 2
Soaking Pit
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Test No.
Date
Time
Pit Temp., °P
North Pit Temp., °P
Burner Position Control
Pit Pressure, in. H.,0
Battery Gas Press., psig
Flue Press. , in. H.,0
Gas Flow Indie., CFH x 300
Air Flow Indie., CFH x 3000
Fuel/Air Ratio Control
Total Gas Flow Indie.
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-------
OPERATING DATA
Location 16
Unit 2
Soaking Pit .
Test No.
Date
Time
Pit Temp. , °F ;
North Pit Temp., °F
Burner Position Control
Pit Pressure, in. H,O
Battery Gas Press., psig
Flue Press. , in. H,O
Gas Flow Indie., CFH x 300
Air Flow Indie., CFH x 3000
Fuel/Air Ratio Control
Total Gas Flow Indie.
(Two Pits)
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OPERATING DATA
Location 16
unit 2
Soaking Fit
Test No.
Date
Time
Pit Temp., °P
North Pit Temp., "P
Burner Position Control
Pit Pressure, in. H.,0
Battery Gas Press., psig
Flue Press. > in. H.O
Gas Flow Indie., CFB x 300
Air Flow Indie., CFH x 3000
Fuel/Air Ratio Control
Total Gas Flow Indie.
(Two Pits)
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-------
TECHNICAL REPORT DATA
(Please read Instructions on the reverse before completing)
1. REPORT NO.
EPA-600/7-79-015c
2.
3. RECIPIENT'S ACCESSION NO.
4. TITLE AND SUBTITLE
Application of Combustion Modifications to Industrial
Combustion Equipment (Data Supplement B)
6. REPORT DATE
February 1979
6. PERFORMING ORGANIZATION CODE
7.AUTHOR(S) K.T.Fisher, H.J.Buening, W.A.Carter,
P.K.Engel, S.C. Hunter, and R. J. Tidona
8. PERFORMING ORGANIZATION REPORT NO.
KVB 6002-734a
9. PERFORMING ORGANIZATION NAME AND ADDRESS
KVB, Inc.
17332 Irvine Boulevard
Tustin, California 92680
10. PROGRAM ELEMENT NO.
EHE624A
11. CONTRACT/GRANT NO.
68-02-2144
12. SPONSORING AGENCY NAME AND ADDRESS
EPA, Office of Research and Development
Industrial Environmental Research Laboratory
Research Triangle Park, NC 27711
13. TYPE OF REPORT AND PERIOD COVERED
Supplement; 1/76 - 1/78
14. SPONSORING AGENCY CODE
EPA/600/13
IB. SUPPLEMENTARY NOTM .jERL-RTP project officer is Robert E. Hall, MD-65, 919/541-
2477.
. ABSTRACT
SUppiement provides raw data from a study of the effects of combustion
modifications on air pollutant emissions from a variety of industrial combustion
equipment. Tested were 22 units, including refinery process .heaters; clay and
cement kilns; steel and aluminum furnaces; boilers burning black liquor, woodbark,
and CO gas; internal combustion engines; and gas turbine combined cycles. Prjocess
variables, fuel types, excess air reduction, burner adjustments, and staged cbmbus-
tion were evaluated primarily for their effect on NOx emissions. Emissions ofj NOx,
SOx, CO, and HC were measured on all units. Emissions of particulate mass and
size, trace species, and organics were measured on selected units. This dataj
supplement is intended for researchers who wish to perform their own detailed
calculations.
17.
KEY WORDS AND DOCUMENT ANALYSIS
DESCRIPTORS
b.lDENTIFIERS/OPEN ENDED TERMS
c. COS AT I Field/Group
Air Pollution
Combustion
Boilers
Furnaces
Nitrogen Oxides
Dust
Fossil Fuels
Particle Size
Chemical Analysis
Industrial Processes Stationary
Gas Turbine Engines Combustion
Reciprocating En-
gines
Organic Compounds
Inorganic Com-
pounds
Air Pollution Control
Sources
Modification
Particulate
Excess Air
Staged Combustion
13 B
21B
13A
07B
11G
21D
MB
07D
13H
21E
21G
07C
18. DISTRIBUTION STATEMENT
Unlimited
19. SECURITY CLASS (ThisReport)
Unclassified
21. NO. OF PAGES
443
20. SECURITY CLASS (Thispage)
Unclassified
22. PRICE
EPA Form 2220-1 (»-73)
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