72-CI-28 (GRN)
SOURCE TEST REPORT
ON MEASUREMENT OF EMISSIONS FROM
CARGILL, INC.
SIOUX CITY, IOWA
FOR
ENVIRONMENTAL PROTECTION AGENCY
UNITED STATES GOVERNMENT
THOMAS E. WARD
PROJECT TEST OFFICER
engineering, im:
2324 S. W. 34th STREET / GAINESVILLE, FLORIDA 32601 / PHONE 904/372-3318
-------
72-CI-28 (GRN)
SOURCE TEST REPORT
ON MEASUREMENT OF EMISSIONS FROM
CARSILL, INC.
SIOUX CITY, IOWA
FOR
ENVIRONMENTAL PROTECTION AGENCY
UNITED STATES GOVERNMENT
THOMAS E. WARD
PROJECT TEST OFFICER
-------
SOURCE TEST REPORT
PLANT TESTED: Cargill, Inc.
Sioux City, Iowa
TESTOR: Environmental Engineering, Inc.
2324 Southwest 34 Street
Gainesville, Florida 32601
CONTRACT NO: 68-02-0232-Task Order 9
-------
TABLE OF CONTENTS
Page No.
Introduction 1
Summary of Results 2
Location of Sampling Points 8
Sampling and Analytical Procedures 16
Appendices
A. Particulate Emission Calculations
B. Plant Operating Data
C. Field Data Sheets
D. Complete Sampling Procedures
E. Field Test Log
F. Project Participants
-------
INTRODUCTION
Particulate emission tests were performed on three separate
sources located at the Cargill, Inc. Feed and Grain Mill in Sioux City,
Iowa. The testing was performed during the week of June 19, 1972.
The sources tested were the Hammer Mill, the Column Cooler
inlet and outlet, and the Pan Cooler inlet and outlet.
All three sources were controlled by cyclonic dry dust col-
lectors. Three, two-hour tests were performed on each of the five points,
-------
SUMMARY OF RESULTS
Summarized results of the particulate emission stack tests
performed at Cargill, Inc. are included in Tables 1-5.
The Environmental Protection Agency (EPA) performed the
analyses.
Complete particulate emission calculation data are included
in Appendix A.
Complete plant operating data collected by the EPA are in-
cluded in Appendix B.
-------
S.QURC& TE&Z
TABLE 1
TEST HO '-EPA 72-CI-28 (CRN} f]Q OF RUNS - 3
PLA11T - CAP GILL SIOUX CITY, IOI/A
SOURCE - UAm2YiL 7/20 COLLECTED, ML ilj28 i-jll i_25. ป-
11) VOL H20. VAPOR COLLECTED, S.T.P. , CU FTJLJNA.- 1_JMLซ J.J1/L.^__
12)Sr/iC^ 6V15 MOISTURE, PERCENT VOLUME 1_JLJL_ .-l^-S i_^5
13)ASSUMED. STACK GAS MOISTURE, PCT VOL i_JLJL ___i_JL.-3 1__2_,.3
1S)PERCENT 02 1_ZEI 1 "T !__"____
17) PER CENT N2 lI!rIII~IIIlIIE^I__IiII-rIIII
1*)PERCEHT EXCESS AIR , STACK GAS WAS AIR 1_JNA . 1 N/L ._1__NA_
19)MOLECULAR I/EIGHT OF STACK GAS, DRY i_JL8_ซ_8JL l__2JjjJ____l^JJjJJ.
20)HOLECULAR VEJGHT OF STACK CAS, STK COA'Z?1__2_8_-JL l__28jj l_.28_..5j?_
21)5^67^ GAS SPECIFIC GRAVITY 1__ฐ_-JL9_ l__0_.JJ_____i__ฐ_:.?JL-
22MVG SQUARE ROOT (VEL HEAD), IN H20 1__ฐ_'_2_5_ J.JL'JJJ?- JLJL-H2-
23)/lFZiYMG'ฃ' 5^0^ ^5 TEMPERATURE, DEG F 1__8_5_'JL I-JIL-.2 1_J?J?_:J:_.
2H)AVG-SQUARE-ROOT (STK TEMPxVEL HEAD) i^A'JJtL i__6_-^ l_J_:JkงJL
2 5)PITOT CORRECTION FACTOR l__ฐ_-_8_3_ .L-JL-JliL __l_.?j:JJ_.
26)52^0^ PRESSURE, IN HG, ABSOLUTE 1_ 2B_'_6_._ .l-JJ-'JJ- l_J?JL:.liL
27)STACK GAS VEL, STACK COND, F.P.M. i_ZLB_'__ 1__9_5J_ซ_3 1_J?.^
28)STACK AREA, SQ FEET 1__4 2_L 1^-- - ll:.2.-8.
29)EFFECTIVE STACK AREA, SQUARE FEET 1_42___. 1__3-.'J?J? 1
30)5r/iC'X 016' FLOW RATE, S.T.P. , SCFMD ' 1_^?JL 1__2A5IJ 1
3l);i/2i"i"' i''Ji'i'i' OF TEST, i-illiUTES . I.., -.J _L__9JL.QL_ 1_77. .
. 32)SAMFLItiG NOZZLE UlA/JETER, INCHES . 1__E^ZZ^_ 1__?J_J__ 1__:__ป
33)P.ERCENT ISOKIa'ETIC i__ll.'Z. l-JOO/9. _L1QO.._0_-.
34JPARTICULATE -EMISSIONS '@ S.T.P., lb/hr
FRONT HALF 0.06 0.07 0.05
BACK HALF 0.02 0.03 0.03'
TOTALS - 0.08 0.10 0.09
***,b'.r.P.<--> DRY, 70 DEGREES F, 2S . 9 2 Hi CUES MERCURY***
*Based upon wet and dry bulb thermometry
3
-------
T.ES.T
TABLE 2
'TEST NO - EPA 72-CI-2B (CRN) HO OF RUfS - 3
PLAIT T - CARGILL SIOUX CITY, IOUA
HOURCE - COLUlitl COOLER III LET
vypp, OF PLAfJT - FEED AND GRAIN MILL
CONTROL EQUIPMENT - DRY CYCLONIC DUST COLLECTOR
POLLUTANTS SAMPLED - PARTICULATES
1)RUN NUMBER
2) DATE
3) TIME BEGAN
H)TIME END
5)BAROMETRIC PRESSURE, IN 11 G
&)METER ORIFICE PRESSURE DROP,
i ____ 1__ ____ 1
l_JVJI27-7-2._i
i__L7_i-2JL ___ 1 __ OJL:_5J1
IN HG
7) VOL DRY GAS METER COND, CUBIC FEET
8) AVERAGE GAS METER TEMPERATURE, DEG
V)VOL DRY GAS, S.T.P. , CUBIC FEET
Q) TOTAL H20 COLLECTED, ML -
l__2Ji-JL1__ __ 1 __ 2.&._a. ____ 1_JL8.-J?
1.JLJ1 ______ 1 __ QLJU_ ____ l__ฐ_-3
1_JฑJLJIX1_ __ 1 __ t5.*.S_2JL __ JL.5J?_s.JjL:
1_JL2_JL ____ i __ TJLJL ___ _1__?JL __ :
i_JL3_Jt _____ 1 __ t'U.QJSJ'L __ l_3JbJ?.:}J
1__35. ______ 1__35 _______ 1-^5
H20 VAPOR COLLECTED, S.T.P. , CU FTl_M- ____ ___ 1 __ N& ___ .; ___ 1-_NA-
12)S!TACX GAS MOISTURE, PERCENT VOLUME
13) ASSUMED STACK GAS MOISTURE, PCT VOL
lH)PERCEtiT C02
02
CO
N2
1B)PERCEHT EXCESS AIR ,
1B)MOLECULAR WEIGHT OF
2Q)MOLECULAR WEIGHT OF
21)SฅACK GAS SPECIFIC
*
1
i
1
L^L
L_5
3'
1
1
3.^.5.
1
1_J_-
JL_"
16) PERCENT
17)PERCEnT
STACK GAS WAS AIR
STACK GAS, DRY
STACK CAS, STK
GRAVITY
22)AVG SQUARE ROOT (VEL HEAD), IN H20
23) AVERAGE STACK GAS TEMPERATURE, DEG F
2H)AVG SQUARE ROOT (STK TEMPxVEL HEAD)
25) PI TOT CORRECTION FACTOR
26)STACK PRESSURE, IN 'EG, ABSOLUTE
2 7 ) STA CK GAS VEL , STACK COND , F.P.M.
.2B) STACK AREA, SQ FEET
29)EFFECTIVE STACK AREA, SQUARE FEET
30) STACK GAS FLOW RATE, S.T.P. , SCFMD
31) MT TIME OF TEST, MINUTES
NOZZLE DIAMETER, INCHES
__ . -
1 __ ~~ ______ .1 __ n-- _______ L__"
1 __ ~~ ______ 1 __ Z- ____ ___ JL_"___
1__-JNA__ ____ 1__NA ______ 1__NA_
i__!R_ซ_8JL_ __ 1 __ 28_._8_5____J____2_8_._8_5
COND]._JJL.^ ___ ._! __ 28J4_6____J_ _28_. U_6
1__0_._9JL ____ JLJL-JL?. ____ 1_.ฐJ^
1_JL'JLฐJL ___ i __ \.'-?J^- ___ i_" '
I^IAJL'J. ___ i__U.!'JL ____ lซ
i__3JL'_2_5JL __ 1 __ !1/JL17_ __ 1_ __.
JLJL'JL3- ____ 1 __
-------
SOURC& l'ฃSI fid ฃ4
TABLE 3
TEST NO - EPA 72-CI-2B (GRN)
PLANT - CAP GILL SIOUX CITY, 10 UA
SOURCE- - COLUMN COOLER OUTLET
TYPE OF PLANT - FEED AND GRAIN MILL
CONTROL EO.UIPMENT - DRY CYCLONIC DUST
POLLUTANTS SAMPLED - PARTICULATES
NO OF RUNS - 3
COLLECTOR
1)RUN NUMBER
2)DATE
3) TIME 'BEGAN
>l)TIME END
5)BAXOMETRIC PRESSURE , IN HG
6)METER ORIFICE PRESSURE DROP, IN HG
7) VOL DRY GAS METER COI'ID, CUBIC FEET
8) AVER AGE GAS METER TEMPERATURE, DEG F
<})VOL DRY GAS, S.T.P. , CUBIC FEET
10) TOTAL H20 COLLECTED, ML
11) VOL H20 VAPOR COLLECTED, S.T.P. , CU F
12)STACK GAS MOISTURE, PERCENT VOLUME *
13) ASSUMED STACK GAS MOISTURE, PCT VOL
1H)PERCENT C02
IS) PERCENT 02
1S)PERCENT CO
17) PER CENT H2
1B)PERCENT EXCESS AIR, STACK GAS WAS AIR
19)MOLECULAR HEIGHT OF STACK GAS, DRY
20) MOLECULAR HEIGHT OF STACK GAS, STK CON
2DSTACK GAS SPECIFIC GRAVITY
22)AVG SQUARE ROOT (VEL HEAD), IN H20
23) AVER AGE STACK GAS TEMPERATURE, DEG F
2^)AVG SQUARE ROOT (STK TEMP'
i 8 2_, 7_5 f
1 7 9_. \_
I 59
?P \ MA
1 3- 3
J "
1 "
JL-
1 --__
1 NA
_[ 28.85
D^ 28.48
J_ 0.98
J_ 0.674
_[ 1 0 4 . G
J_ 16. DOS
ฑ 0.83
_[ 28.9
j TB"7 3 .1
i T"-"75
J.__''
1 -,_ ' "
J^ TUT
i rm~.~/i~
j. _ _
0.. 23
0.37
1
j_
j_
1
_[
> j_
1
1
j^
_[
1
I
1
1
I
1
j^
_L
1
I
_[
I
i- j_
I
1
_[
___!
^ i 3 __
J17_:_5J3 1 3-1:11
0_g_. 4j _[_ 14:06
-2JL.J _1 28' B
70_,484 J. 86.51
R8^.J 1 86.1
pp 24J 1 81.199
55 i 63
CsIA 1 JslA.
3_i J 1 ^ 5
3_, 3 _[ 3 . 3
-- 1 --
J[ -
_i " _
i __
HA. 1 _NA_
28.85 J, 28.85
28.45 J_ 28 ,T?
0.98 1 0."9"B
0.604 1 "0."?T-
108". 5 ~| IT^T ~ '
0. 83 J[ D/F3
28.8 | "2T5 ."B
2139.1 i V.b'27 .^2
* J.
11 Q c i TfTTTS
H . O ,J 1 r . ^ ^
^D"4l ฑ "9T1T.T)
J_
* j^ ^
0.35 0.22
0. 29 0.17
0.63 0.38
***S.T.P.+-> DRY, 70 DEGREES F, 29.92 INCHES MERCURY***
*Based upon wet and dry bulb thermometry
5
-------
SOURCE
TABLE 4
-TEST NO - EPA 72-01-28 (GRN) NO OF
PLANT - CAP GILL SIOUX CITY, IOUA
SOURCE - PAN COOLER INLET
TYPE OF PLANT - FEED AND GRAIN MILL
CONTROL EQUIPMENT -
POLLUTANTS SAMPLED -
DRY CYCLONIC
PARTICIPATES.
DUST COLLECTOR
1)RUN NUMBER
2) DATE
3) TIME BEGAN
H)TIME END
5)BAROMETRIC PRESSURE, IN HG
6)METER ORIFICE PRESSURE DROP, IN HG
7) VOL DRY GAS METER COND, CUBIC FEET
8) AVERAGE GAS METER TEMPERATURE, DEC F
B)VOL DRY GAS, S.T.P. , CUBIC FEET
10) TOTAL 1120 COLLECTED, ML
1DVOL H20 VAPOR COLLECTED, S.T.P. , CU I
12) STACK GAS MOISTURE, PERCENT VOLUME *
13) AS SUM ED STACK GAS MOISTURE, PCT VOL
in) PER CENT C02
15) PER CENT 02
16 )PER CENT CO
17) PER CENT N2
18) PER CENT EXCESS AIR , STACK GAS WAS AIR
13)MOLECULAR WEIGHT OF STACK GAS, DRY
20)MOLECULAR WEIGHT OF STACK GAS, STK C01
2DSTACK GAS SPECIFIC GRAVITY
22)AVG SQUARE ROOT (VEL HEAD), IN H20
23) AVERAGE STACK GAS TEMPERATURE, DEG F
2*)AVG SQUARE' ROOT (STK TEMP*VEL HEAD)
2 5) PI TOT CORRECTION FACTOR
26)STACK PRESSURE, IN HG, ABSOLUTE
27) STACK GAS VEL, STACK COND, F.P.M.
2Q)STACK AREA, SQ FEET
2B)EFFECTIVE STACK AREA, SQUARE FEET
30) STACK GAS FLOW RATE, S.T.P. , SCFMD
.3DNET TlilE OF TEST, MINUTES
32)SAMPLING NOZZLE DIAMETER, INCHES
3 3) PERCENT ISO-KINETIC
34) PARTICIPATE EMISSIONS @ S.T.P., Ib/hr
F-ROIJT HALF
.BACK HALF
TOTALS
1 JL.
i _&V/L2JVJL:
1 6_iJxP
*
1 _2A^_7JL
i .JLJlfL..
1 711
i _ULJL^J13J
i 66
7T\ I^A
1 ฐ 7
1 2 J> _
1 -
1 " __
1
i " -
1 NA
J_ 28.85
'/ฃ>! 28.56
i 0. 99
_]_ 0.905
1 95 9
1 21 . 335
J_ 0.83
1 29
J_ 3153.1
1 3 69
J_ 3.69
i .1 0 4 5 7
J f2"0
I ฐ~ซ 2~^
j_ 98". 5~
133.65
:0. 05
133.69
J_
, _L
1
1
j
j_
i _[
j^
2_ 1
_[
_[
j_
j_
1
I
I
I
I
|
j_
j_
j[
_[
I
j_
1
j_
I
j_
j_
j^
r)
ฃ7 12 >13
JL'Ji^_ _
11 ;05
_28__9_ .
jL'iJLJiSJl
6_9_ซ_6_
1 liJL.J'- 8 ']
82_
NA
2 7
2.^.6
__
-NA
28.85
28.56
0 ^ 9
1 095
90
25.675
0. 83
29.1
3788.1
3.69
3.69
12750
TTO "" "
(T. 2~5~
TOO. r
248. UU
0. 08
248.52
i 3_
1 1 c-l 2 2_/ 7 2
J. 12:30
1 1 H : 3 5
i 28.91
i 4.32
J_ 142.783
L 75.9
1 137.955
_ 1 30 _
1 _NA_ -
_[ 2.7
1 2.6
1 "
1
1
i
1 NA
J_ 28. 85
J_ 28.56
1 0.99
j^ 1.066
i 9~9~. 3~
~ J_ 25". 202 "
I o~.in~
- i IT. r "
1 *3 / JL o , O
| :i. h9
1 3 .^^r
1 , "'
"" i i'zu
1 "iT.~?U~
j_ lul.l
242.35
0.11
242 M 7
***$.'!'.P.<--* DRY, 70 DEGREES F, 29.92 INCHES MERCURY***
*Based upon wet and dry bulb thermometry
6
-------
SOURCE TE&T
TABLE 5
TEST NO - VPA 72-CT-28 (CRN) NO OF RUNS - 3 :
PLANT - CARGILL SIOUX CITY, IOWA
SOURCE -PAN COOLER OUTLET
TYPE OF PLANT - FEED AND GRAIN MILL
CONTROL EQUIPMENT - DRY CYCLONIC COLLECTOR
POLLUTANTS SAMPLED - PARTICULARS
1 )RUU NUMBER
2)DATE
3) TIME BEGAN
H)TIME END
5)BAROMETRIC PRESSURE, IN EG
&)METER ORIFICE PRESSURE DROP, IN EG
1)VOL DRY GAS METER COND, CUBIC FEET
8) AVER AGE GAS METER TEMPERATURE, DEC F
9) VOL DRY GAS, S.T.P. , CUBIC FEET
10) TOTAL H20 COLLECTED, ML
11)701 H20 VAPOR COLLECTED, S.T.P. , CU F1.
\2)STACK GAS MOISTURE,. PERCENT VOLUME*
13) ASSUMED STACK GAS MOISTURE, PCT VOL
iH) PER CENT C02
IS) PERCENT 02
IS) PERCENT CO
17) PER CENT ti 2
18)PERCENT EXCESS AIR , STACK GAS WAS AIR
19) MOLECULAR I/EIGHT OF STACK GAS, DRY
20)!-10LECULAR HEIGHT OF STACK GAS, STK CON>
21) STACK GAS SPECIFIC GRAVITY-
22)AVG SQUARE ROOT (VEL HEAD), IN H20
23) AVER AGE STACK GAS TEMPERATURE, DEG F
2H)AVG SQUARE ROOT (STK TEMP*VEL HEAD)
2 5) PI TOT CORRECTION FACTOR
2$) STACK PRESSURE, IN HG, ABSOLUTE .
27) STACK GAS VEL, STACK COND, F.P.M.
2B) STACK AREA, SQ FEET
29)EFFECTIVE STACK AREA, SQUARE FEET
3Q)STACK GAS FLOW RATE, S.T.P. , SCFMD
31) NET TIME OF TEST, MIl^U^ES
32) SAMPLING i>OZZLE DIAMETER, INCHES
3 3) PERCENT ISOKINETIC
34) PARTICIPATE EMISSIONS @ S.T.P., Ib/hr
FRONT HALF
TOTALS
1 JL
i_JI/J>J_/JJL_
JLJULL5A.
hiM8::::
i 73<_6
i Jฃ6
yj_ M/\
1 '2.1
i 2
i
i _. "
1 --
1 NA
J_ 28.85
r>J_ 28.63
J_ 0.99
J_ 0.447
i ^"8< 7
j_~ TO. 46 9
I 0. 83
J ~28~.T8 ~
1 " _
J -9T5TT
i 9~.~5T~
| TTU2T"
"1"! 7 . b
V 0 . 'A b
1 TDTT."T
l'S.07
0.29
15.36
1
l~"
|
|
f
I
I
I
1
1
I
1
!
1
1
1
1
1
1
1
1
1
1
1
2
-8-4-iu5__
_2_n_ojF_
-1_^L5_
.-' 1 _3_ ' ' '
i_2JLJU _-:
. _ IJLJJ
_7J1~_7_ i 83_^5
33- __
-?.,! ,
0
__
--
NA
2j> ^ 5
25.^.63
0 t_99
0. 545
89.1
12.76
0. 83
28.91
1887.
9.51
9. 51
1 G 3 9 3
120
0.25
105.4
21. 86
1.01
22.87
. Il 34 *""!
!'?*_!
1 2
i
1
i "
1 NA
J. 28.85
J_ 28.62
. -1_ฐ'99_
_[ 0.552
J_ 97 . 2
9 J_ 13.029
J_ 0.83
1 28.91
9 I f9 2 6~. 5"
~jj 9.5f "
._ J. *
I T70"
i D"'75"
(^ TOT
9.32
'0.40
'9.72
***i>'. i1. P. <--! DRY t 70 DEGREES /', 29.92 INCHES MERCURY***
*Based upon wet and dry bulb thermometry
7
-------
LOCATION OF SAMPLING POINTS
Sampling ports and points were selected by using the guide-
lines stated in Method 1 of the Federal Register (36. F. R. 24882,
24883, December 23, 1971).
Figures 1-8 are diagrams of the sources sampled.
Table 6 is the location of sampling points for each source.
8
-------
Hammer Mill
Exhaust
Column Cooler
Exhaust
\ Penthouse
\
\
\
\ . .
\
Pan Cooler Inlet
Rail in
O
Interior of bldg.
\
\
\
N
\
\
^
Figure 1. Top View of Roof at 4th Floor Level
-------
Stack Extension (28" I.D.)
Straightening Vanes "*
it-Roof ~~
12" I.D.
Whole Corn
No. 2 Yellow
Whole Corn
No. 2 Yellow
7-7r~777rf77?77 1 7 r 7
Bin No. 6
Pulverized
. Corn
Bin No. 5
Pulverized
Corn
Figure 2. Hammer Mill System
10
-------
/-Roof
r
5th Floor
FT"?
LiJ
Straightening Vanes
13.
Inlet
Sampling Site
(26" I.D.)
/~4th Floor
t
Return
to
Pellet Mill
California Pellet Mill
Pan Cooler
Figure 3. Pan Cooler System
11
-------
/-Roof
r /? v '7~7~ 7"~r ~
Inlet
Sampling Site
(16 7/8".I.D.)
(3rd Floor *
;/./... y /_|J7""/.""7|~./ ;y -77-7-
< Stack Estension (29V I.D.)
ซa?
< Straightening Vanes
r'J^"^7. _J ~J
16"
/ X / / / /'
Return to
Pellet Mill
Floor
\f /_./ f f /^f / / 7 / /
Basement
Fan
California Pellet Mill
t f ' f f /' I LsL. /.<*, J, ?,,{, /.,
r~7
i.
Vertical Cooler
Figure 4. Column Cooler System
12
-------
i
80"
i
60"
r \
*
16"
t
44"
f *
l
V
28" I'.D.
1 1 .
1 1 "I
1 1 1
L__L_J
( Stack . - .
OR" f "ป-^~ Extension
ป I
^^^--^ Sample Ports
(2 at 90ฐ)
^^ Straightening vanes
./^ (2 panels at 90ฐ, 21" x 28")
^ ^ Roof at 4th floor level
Figure 5. Hammer Mill Exhaust
Roof at 4th floor level
Curb
(
) Cut-out ^
/ in roof
^
26" I.D.A X,
-*. A /
-*. \^/
o
18" ^^
^^
.4 3ฐ" t-
-G F-
* '
-, Sa
1 (2
13
ro
80
gr
Interior of bldg.
Sample PorM;s
(2 at 90ฐ)
13" above
roof level,
80' above
Y/"/'
Figure 6. Pan Cooler Inlet
13
-------
Sample Ports
(2 at 90ฐ)
42"
I5CXIXIC03^
Straightening Vanes'-z~4i
(2 panels at 90ฐ, 22"x29V)
Interior of
Cyclone
1 f
.
36
Stack Extension
27"
\\x\\\
29V I.D.
rvv
100"
Roof at 4th
Floor Level
Figure 7. Column Cooler Exhaust (Side View)
c
... \ \ \\\ \ v\\\
/~\
\j
r~ i~ i
i ii
, i r
L_ i i
^41 3/4" I.D.^
18"
30"
\\\\\\\\\\\\ -^
^Straightening Vanes ^~"
(2 panels at 90ฐ, 31"x41 3/4")
Top
Roof
Figure 8. Pan Cooler Exhaust (Side View)
14
-------
TABLE 6
Location of Sampling Points
^x. Points
Source ^\.
Hammer Mill
Column Cooler
'(Inlet)
Column Cooler
(Outlet)
Pan Cooler
(Inlet)
Pan Cooler
(Outlet)
1
$
1
-1
'i
',f
2
4
ซ1
'!
'ซ
',!
3
'1
5
1 8
7U
19
2 64
4
'i
ปi
, 21
f 64
18 If
, 19
3 64
5
ซ*
"i
3ll
22 T6
*!
6
3^
ปt
3 29
J 32
24 27
^ 32
4
7
'1
ซf
*
8
5 32"
i
li
Distance From Inside Stack Wall
9
fc
I
'I
10
'1
ซfe
"i
11
t
9i
131
12
"t
ซ
"!
"I
13
ปi
"!
"1
14
19
"i
-t
15
20 If
21 If
3ฐi
16
21 32"
23
" 32
,, 9
J> 19
22 32
r\>
CO
ojiro
rojtn
21
33 32
18
"i
ปl
35
19
"i
ปs
-ป
20
25
7K 13
26 32
ป!
21
ซ 13
25 T6
?7
" 64
is 29
38 64
22
-fe
27 7
27 8
39^.
Jy 64
23
9fi 7
25 IB"
"1
ซjง
24
ปTT
ปi
40 3?
-------
SAMPLING AND ANALYTICAL PROCEDURES FOR
PARTICULATE EMISSIONS FROM STATIONARY SOURCES
The method used was Method 5 of the Federal Register (36 F.R.,
March 31, 1971), Determination of Participate Emissions From Stationary
Sources.
The complete description of the sampling method used is in
Appendix D.
The EPA performed the sample analyses.
16
-------
APPENDIX A
Participate Emission Calculations
-------
E.E.I. SOURCE SAMPLING 'NOMENCLATURE SHEET
PB - Barometric pressure, inches Hg
PS - Stack pressure, inches Hg
As - Stack area, sq. ft.
AS1- Effective area of positive stack gas flow, sq. ft.
NPTS - Number of traverse points where the pitot velocity head was greater than zero
TS - Stack temperature, ฐR
TM - Meter temperature, ฐR
t[ - Average square root of velocity head, //inches ^0
AH - Average meter orifice pressure differential, inches H20
AN - Sampling nozzle area, square feet
CP - S-type pitot tube correction factor
VM ~ Recorded meter volume sample, cubic feet (meter conditions)
VC - Condensate and silica gel increase in impringers, milliliters
Po - Pressure at the dry test meter orifice, |~PB +A. if] inches Hg
L 13
STP - Standard conditions, dry, 70ฐF, 29.92 inches Hg
Conversion of condensate in milliliters to water vapor in cubic feet (STP)
Volume sampled, cubic feet (STP)
Total water vapor volume and dry gas volume sampled, cubic feet (STP)
Moisture fraction of stack gas
Dry gas fraction
Molecular weight of stack gas, Ibs/lb-mole (dry conditions)
Molecular weight of stack gas, Ibs/lb-mole (stack conditions)
Specific gravity of stack gas, referred to air
Excess air, %
Average square root of velocity head times stack temperature
Stack gas velocity, feet per minute
Stack gas flow rate, cubic feet per minute (stack conditions)
Stack gas flow rate, cubic feet per minute (dry conditions)
Stack gas flow rate, cubic feet per minute (STP)
Percent isokinetic volume sampled (method described in Federal Register)
Particulate Lab Analysis, grams
Particulate Concentration, grains per standard cubic feet
Particulate Emission Rate, pounds per hour
-------
L
ENQLilUSRlllS, LU.CQP.ZQS.AZm
'MS CALCULATIQUS
PLANT- CAPCILL SIOUX CITY, I0.V4 DA.TF- 6/20/72
STACK- PAWERVILL OUTLF.T RUN 1 FP.O-" 20:30-23:02.5
UF.A7TIF.R CONniTIOt'S- CLFAP AND COLD PP - 28. P I" FfJ PS- 28.6 177 HO
AS'- 3.38 SO. FF.FT TS- 5'J5.3 DKOR^FS R. TM- 5 26 . 8 DF.KRFFS R ซ- 0.25 I-".' 7/2^
. AW- 1.4 J7;7 P20 4ป7- 0.000767 ,9(3. FF.F.7 CP- 0.83 W- 58.645 CF~ VC-2.8 MT>
TOTAL TIMF- 95 Mil? NPTS- 38 ORSAT'. /$/ฃ
i)vt-/v = 7o. o474TxIT'6"'T i3 2^! ICE.
2)VSTPD= ( ( 530)x( K/'/)x (PS + ( A^f I3 6 ) ) )T( 29..92XTW ) 2.) 5.fi^60S. S_CF_
3)W = (W//) + (VSTPD) "".-' 3) !Vn.__.. SCF,
= ( WV) * ( 1/T) 4) Qj.02.3
= d.o - v) 5)IJLaz.! !
6)ASSUMED MOISTURE FRACTIOil 6) 0..023
T)MD = (.4txC02) -h (.32x02) + ( . 28x (CO + //2 ) ) 7) 28._85
= (MS) T (28.99) 9) oZi^IZIIIIIII!
10)ฃ,^ = (100)x(Q2-0. 5xCQ)v( _(.g_._266x//2)-(Q2-0. SxgQ) ) 10)__|LA %.
13)CS = (If) x US') ' 13)ZZIi'H.
x (FDA) 14)__287_3_
x ( 530^^5 ) x (PSv29.92) 15) 26_6_q_
16)PI6"0 = ( (0. OQ2b7xVCxฃฃ) + (poxฃฃxVM*T,ti) ) * ( TIMExU_xPSxAa ) 16)__9Q.i.5_ ^__
17)c'6'i'P = ( 15.43xy ) v "(VSU-PD) UNITS : GRAIL'S/SCF
18)i'12 = ( 12xES'J'P ) T (^C'02) y//Jr5 : 'GRAINS/SCF
19)i'50 = ( ฃSrpx(ioO+E/l) ) * (150) [///ITS : GRAIliS/SCF
20)EM = (O.OQBS7)x(ESTP)x(QSTPD) " UNITS : POUNDS/HOUR
l>ARTIclJlAli'iri^AB~jKA^^
FRONT HALF - .0098 .0027 0 06
SACK HALF - .0038 .0010 o!o2
TOTALS - .0136 .0037 o!o8
. 1_ . 1 .
COMMtltiTS :
CONDUCTED By : ._
"~~~ ~~ \Af^\J^ ) environmental engineering, int:
-------
mQ.lliHZB.LRQ> lV.CQ.Rr.QRA.ZEU
PLANT- GAR GILL . SIOUX CITY, IOWA DATE- 6/21/72
STACK- HA11MERMILL OUTLET. mill 1 FROM 9 s 55-11-45
LEATHER CONDITIONS- CLEAR AND COLD PB- 28.78 If] HG PS- 2R.78 in HG
AS1- 3.38 SO.. FEET TS- 545.2 DEGREES R. TV- 522.2 DEGREES R H- 0.276 If] 7/20
A77- 1.67 111 1110 Afl- 0.000767 SQ. FEET CP- 0.83 V!<- 65.517 CF VC-3S. ML
TOTAL TIME- 3ฃ MI/7 WP2V7- 38 ORSAT-. " '
1)VUV - To. 0474TxTl/C)
2)VSTPD = ( ( 530)x( y/4Ox(P3-t-( A#*13 . 6) ) )T(
3)Fi' = (WK) + (VSTPD) ' ' 3)___^/ฃ. SCF.
4)>/ = (VW) * (V21) 4) ;D^.D2J2
5)FZ?/i = (1.0 - ป/) 5)__j}J.522
6)ASSUMED MOISTURE FRACTION 6) ฃ^Q22
'/)MD = (,44xC02) t (.32x02) + ( . 28x (CO + N2. ) ) 7) 2S-.B.5.
9)Gฃ = (MS) T (28.99 ) 9) 0^52
= (100)x(Q2-0. 5xCQ)4( (0. 266x/;2 )-(02-0. 5xCQ) ) 10) j^A S
)*AVG( JdlxTS) ) 12)~isH^H~IIlฃPif
13) 3226 ACFM
14) CO = (QS) x (FDA) . 14) .316.1 CKL1!2
x ( 530 *ฃg ) x (ZJSv29.92) 15) 2956 S.CFU
15.43x/ ) f "( VSTPD) UNITS : GRAIilS~/SCF
18)i,'12 = ( 12*ES'J!P ) * (%C02) UNITS : GRAINS/SCF
19)L'50 = ( ^52'Px(100+z?4) ) v (150) UNITS : GRAIUS/SCF
20)EM = (0. 00857)x(ฃ'Si'1P)x(e52'Pฃ>) UKITS : POUNDS/HOUR
ซ____ _^__ป ^..___ซ.... _ซ.____ ^___M. _^_^^ ^. ^_ซ_^ป- _^ ซ ^ ^ ^- -^ ^ ซ^
T7 J~" /"*/^)<7/^7"'77'7'rP/'71T/0?'Q^/^y /C/'^JT*^ I JTAfTQCT/O/'' *P^ T7 T^1'
i ii (sUiii'ฃ'{vjLS\AJ.J.Ut Or ^ | brJJ. ฃ>O J. U i^ ttJi J. &
__; 1EI2JL
,0120 .0029 ' 0 07
B/CX 7//4LF - .0045 .0011 0*03
TOTALS - _ .0165 .0040 ; . 0]lO
COMMEiiTS : s^L___C
CONDUCTED By : . .
~~~"~~ I^~J/^) ^ ettvinmmcntal cnfjineering, inc.
-------
..I
LRCQRPQRAim
SAliPLIiiG CALCULATIONS
PLANT- CARGILL SIOUX CITY, IOUA DAFF- 6/21/72
STACK- P.AlMF.miLL OUTLET RVH 3 FROM 12:10-13-50
WEATHER COPDITI011S- CLEAR AND COLD PJJ- 28.78 177 P<7 PS- 28.70 1/7 77(7
AS'- 2.76 SQ. FEFT TS- 549.1 DEGREES R TM- 532.8 DEGREES 7? 77- 0 . 20 2 J.'7 7720
AT?- 1.44 IIJ 7/20 /177- 0.000767 ,90.. FEFT CP - 0.03 Wf- 51.093 CF VC-2$ ?'L
TOTAL TIME-77.5 MIH I1PTS- 31 ORSATi Atฃ f-'
- "(0. 0474TxTvf") 1~) lA-A. 5CP.
= (VWV) + (VSTPD) 3) l2^^._. ฃฃฃ.
= C/f/7) T (K21) 4) Q..02.4
= (1.0 - fc') SJ-.O^T.G.
6)ASSUMED MOISTURE FRACTIOil 6 J^O^OS,3
7);'77J = (.44x^02) + (.32x02) t ( . 2 8x (CO + H2 ) ) 7) 2S..2.5.
H)MS = (MD*FDA~) + (18xf/) 8) 2.8^5.9.
9)C5 = (MS) v (28.99)
= (100)x(Q2-0. 5xOO)r( (0. 26 6x772)-(02-0. 5x CO)
'Ctfxi'5) ) = ( l*i;')xSUM( J(fixTS) ) . 11) 6.JL2JL
13)CS = (U) x (/151) 13]
= (QS) x (FDA) 14]
530^^5 ) x (P5v29.92) 15]
) 16)__TOO^O %
= ( 15.43.xJT ) v (VSTPD) UNITS : GRAIiiS/SCF
18)i'12 = ( I'/xESTP ) v (%C02) UNITS : GRAIKS/SCF
19)ฃ'50 = ( ESTP*( 10 0+274) ) * (150) UNITS : GRAIKS/SCF
20)EM = (O.Q08$7)x(ESTP)x(QSTPD) UNITS : POUUDS/HOUR
'ljARyicuT/iT"lAB~^7iATysisl.Mi^^
. FRONT HALF - .0089 .0028 0 05
BACK HALF - .0056 .0010 0*03
TOTALS - .0145 .0046 0-'09
1 _i
COMMEiiTS : ____^.^14!_ 1 '
VAST CONDUCTED By :
^.__-______ _^_ -.^_ .__. ._ /X^A /***^*
If * L-' J envinmmvntal enQiwering* iiw.
-------
ฃ5. UlCQRPQRAT_Ep_
' ZQUdCi; SAVPLI1.C CALCULATIQUS
PLANT- CARGILL SIOUX CITY, IOWA DATE- 6/22/72
STACK- COLUH1! COOLER ItlLET RUN 1 FROf 17:25-19:51
HEATHER CONDITIONS- CLEAR PR- 28.91 IN HG PS- 29.2 in'HC,
AS'- 1.55 SO. FEET TS- 571.5 DEGREES R '' . TM- 549.4 DEGREES R H- 1.307 If! P20
Aฃ- 0.4 IN 7/20 All- 8.5ฃ~5 ,90. FEET CP- 0.83 VM- 46.511 CF VC-3ฃllL
TOTAL TIME- 120 Mill NPTS- 24 OR SAT-. /?//ฃ
1)VWV = (0.0474)x(VC) 1)
2)VSTPD= ( (b30)x( W./)x(pS + (A/7rl3.6)) )v( 29.92x2W ) 2)__43._
3)VT = (VVV) + (75rPO) ' 3).
4)f/ = C/f/V) * (VT) 4).
5)FO/5 = (1.0 - h') 5).
ง)ASSUMtiD MOISTURE FRACTION . 6) P.^.0.!-!.
T)!W = (.44x002) t (.32x02) + ( . 28x (CO + 7/2 ) ) 7 )__2.5.._ง.5_.
9 ) C6" = (MS ) * ( 2 8 . 9 9 )
= (100)x(Q2-0. 5xgQ)v( (0. 266x//2)-(02-0.
~" / -" i \ 1 o ^ 7"l~K*'
< (/ID ) 1JJ ___
x ( 530*ฃS ) x (P5v29.92) 15i
= ( 15.43xy ) T IVSX'PD) ~ ~UUITS : GRAIUslsCF
18)i'12 = ( 12x2i6'i"'P ) t ( %C02 ) UNITS : GRAINS/SCF
19)i'50 = ( ESTPx ( 1QQ+EA) ) T (150) UNITS : GRAIKS/SCF
20)EM = (0.00857)x(sSTP)x(QSTPD) UNITS : POUNDS/HOUR
l>lwTl:l:irLlil^~l^^^
FRONT HALF - 16.8417 5.9877 ' " 330 41
BACK HALF - .0072 .0026 o'l4
TOTALS - : 16.8489 5.9903 32o!s4
COtiMi'ti'fS : _JrLฃ-ฃ ^Jd.^^LL- Jk^ff^5?_^^ ' ' ~
By :
\C~C3 ) vnvimnmenlal engineering, int:
-------
MVIKQ.llllUU.TALMGlu.KERIli.Gt IRCQRPORATM
dQUH_CE sAidPLiuQ Q.&.LCULATIQUS
PLANT- CARGILL SIOUX CTyy, IQUA DATE- 6/23/72
STACK- COLUMN COOLER INLET . RUN 2 FROM 07:50-10:00
WEATHER CONDITIONS- CLEAR . PB- 20.R It! JIG PS- 29 IN JIG
AS*- 1.55 SO.. FEET TS- 573.9 -DEGREES R' TM- 532.4 DEGREES R H- 1.329 in P. 10
AT/- 0.41 IJi 7/20 /[//- 0.5ฃ~5 SO. FEET CP- 0.03 VM~ 45.928 CF ~ VC-3& ML
TOTAL TIME- 120 MItl. NPTS- 24 ORSATi /?/ฃ
_______________ ^- r^/7^2 SCF_
( S30)x( Vl-i) x (PS + ( A/jrlS. 6) ) )ฃ( 29.92xJ'W ) 2) .M-..0.5JJ 5CF_
= (VWV) + (VSTPD) ' 3) ._<#./? 5CF_
= ( W/) i (V21) 4) IL.0.3.R
= (1.0 - k') . 5)__0^96jj
'ISSUMED MOISTURE FRACTION ' 6) JL.jnS.S
= (.44x002) + (.32x02) + (. 28x (00 + 7/2 )) . 7) Jj3^C5
' to)MS = (MDxFDA) + (18x(V) 8) J5^iG ;
9)CS- = (MS) * (28.99) 9) 0.90
10)ฃV1 = ( 100)x (Q2-0. 5xQQ)v ( ( 0. 266x7/2 )-(02-0. SxQQ) ) 10) .M_O 1
12)# = ( 174xOpx (|/(29 . 92vP6'x05) )xAFC( J(H*TS) ) 12).
13)C5 = (i/) x US') 13)__7309 dฃF.y.
= (QS) x (F^i) 14) 2ฐfiH ฃฃL'2.
;= (
-------
'. LU.QQRPQRAZEU. . .
IdVLIHG CALCULATLQUS
PLANT- CARCILL SIOUX CITY, IOWA DATE- 6/23/72
STACK- COLUr'H COOLER INLET RVfl 3 FROM 11:00-14:20
HEATHER CONDITIONS- CLEAR PB- 28.8 177 HG PS- 29 777 PC,'
AS'- 1.55 SO. FEET TS- 577 DEGREES R -.TM- 536 DEGREES R -H- 1.300 177 7720
A7J- 0.4 177 7/20 At!- 8.57?~5 50. FEET CP- 0.83 VU- 46.112 CF VC- ' "
TOTAL TIME- 120 MIN VPTS- 24 OBSAT:
2)VSTPD = ( (b30)x( VM)x(PB + ( A#Tl3.6) ) )*( 29.92x2.W ) 2) J1JU025 ^CF.
3)VT = (VUV) + (VSTPD) 3
4)^ = (VUV) * (VI1) 4!
5)FZM = (1.0 - fc') 5) H^2ฃi
&)ASSUMED MOISTURE FRACTIOll 6).
7)//0 = (.44xC02) t (.32x02) + ( . 28x (CO + //2 ) ) . 7).
;&75) T (28.99) 9).
'. 100)x (02-0. 5xCO)T ( (0. 266x/72 )-(02-0. 5xCO) ) 10).
) = (lT/t')x6't///( J(L'xTS) ) . 11).
;29.92TPSxCS) )x^l/C( y(7/xTS) ) 12).
13)CS = (U) x (/IS1) 13)"
= (^6') x (FDA) 14) 6947.
x ( 530rTS ) x (PS*29.92) 15;~
cSi'P = ( 15.43xJ ) * (VsrP/7) ~ ~UUITS : GRAIiislsCF
%C02) UNITS : CRAIHS/SCF
i9)i'5o = ( fi'si'pxdob+r/i) ) T (150) (///ITS : GRAIUS/SCF
20)EM = (0.008S7)x(ฃSTP)x(CSTP0) UNITS : POUNDS/HOUR
7JARTICuI7lTlTlAB~lllAll(sJs^lJJ^^
FRONT HALF - 11.3295 3.9789 210.90
BACK HALF - . (0043 .0015 o]os
TOTALS - 11.3338 3.9804 210^98
COKMEiiTS : l2.4^1 L^^l.
COtWUCTED By : .
"~""""~~~ ~ ~ ~ \C-"C^ ^ nnrintnmcnfal cnuinffrintf, inf.
\ ^ /
-------
ฃilGIilฃERIUฃ, INCORPORATED.
lldPLIHG CALCULATIONS
PLANT- CARGILL SIOUX CITY, lOh'A DATE- 6/22/72
STACK- COLUMN COOLER OUTLET RV11 1 FROM 17:20-19:45
WEATHER CONDITIONS- CLEAR . PS- 28.9 177 HC, PS- 28^9 III' PC-
AS'- 4.35 SQ. FEET TS- 564.6 DEGREES R- TM~ 539.1 DEGREES R 77- 0.674 Tlj f-!20
A/?- 1.65 J/7 7/20 All- 0.000341 SQ. FEE.T CP- 0.03 VII- 82.758 CF VC-&9 ML~
TOTAL TIME- 110 Mill tlPTS- 44 ORSAT: Alt.
T)VWV = To. 047ปOx'("i'c') l") _i/ฃ2ฃ SCF
2)VSTPD = ( ( 530)x( J/7-/)x (P#-t-( A7/vl3 . 6) ) )*( 29.92x2$ ) 2) TJLJUJi SCF
3)VT = (W/V) + (VSTPD) ~ 3) '^.&A_ SCF
= (WK) T (VT) 4)__0t03_ij.
= (1.0 - (/) 5) 0,_2.6_6_
&)ASSUMED MOISTURE FRACTION 6) P_._0_3_3_
1)MD = (.44xC02) + (.32x02) + ( . 28x (CO + N2 ) ) - 7) 2.8_._8_5_
tilMS = (MDxFDA) + (18x^0 . 8) 2_8_.Jl8
9 ) GS = (MS ) T ( 2 8 . 9 9 )
= ( 100)x (02-0. 5xCQ)v ( (p. 26 6 x//2 )- (02-Q.
KHxTS) )= (lT//)x6-WHi/(//xy5) ) . 11) 1_(1._0_0_9_
13)C5 = (W) x (/io1) 13)HC^CCCI
(FZ>/i)- 14)__99_fiJL__
( 530v?5 ) x (PSv29.92) 15)__?_0_3_9 S.CF.U.
= ( 15.43xy ) f ~(. VSTPD) UNITS : GRAIKS/SCF
18-)i'12 = ( 12xESTP ) * (%C02) .UNITS : GRAINS/SCF
19)i;50 = ( ESTPx(lQQ+EA') ) T (150) UNITS : GRAIUS/SCF
20)EM = (0.00&S7)x(ESTP~)x(QSTPD) UKITS : POUNDS/HOUR
P^i'J^I^i'I^L^B'Tu'xilysISTGYOT"?^^??!?^/!^ Co7/CฃWr^^2'JOA's7c/?7s6T") I S7/J55JOA' fl/^rE
FP0777 77/1LP - .0152 .0030 0.23
RACK HALF - ' ' .0093 .0018 0*14
TOTALS - ' .0245 .0048 o!37
1 1
TEST CONDUCTED BY :
\^C^ ) vnrfnutmt'nlal engineering, int:
-------
MWIQ-MMIAL EHGLu.ZSB.LiiS, LlLQQRPQRAxm
dQUd^L s.6.!dr.L.ฃ.iiQ CA_LCULATXQHS
PLANT- CARGILL SIOUX CITY, IOWA DATE- 6/23/72
STACK- COLUMN COOLER OUTLET RUN 2 FROM 07:50-09:45
WEATHER CONDITIONS- CLEAR AUD COLD PP- 28.8 I A' P.G PS- 28.8 IN JIG
AS1- 4.35 SQ. FEET TS- 568.5 DEGREES R -. TM- 528.7 DEGREES R H- 0.604 r;; 7/2(9
A 77- 1.35 IN T120 AH- 0.000341 ,50. FEET CP~ 0.83 VM- 70.484 CF VC-.ฃ>ฃ l*L
TOTAL TIME- 110 MIN flPTS- 44 ORSAT; /?//C
_______________ _ _ -_ 2^/T gcp
3)VT - (VWV) + (VSTPD) 3) _2ฃ2t SCF
H)U = (VWV) * (VT) 4) Qป.Q.2.7
5)FDA = (1.0 - f/) 5) 0^96,3.
&)ASSUMED MOISTURE FRACTIOil . 6) 0^03.3
= (MDxFDA) + (18xf/) 8)__28..4_5_
9)C5 = (A/S) r (28.99) 9)__0 9Q.
= (100)x(Q2-0. 5xCQ)v( (Q._266x7/2-)-(02-0. SxCO)' ) 10) ฃ/7j %
'"(//xi'S) ) = ( 1 T I!} x S t/.'-7 ( i/ (// x'TS 1 ) . 11) lts.3.9.6
12)i/ = ( 174xt7px (|/( 29 . 92TpSxCS) ) xA VG( y(7/x T5 ) ) 12) 21.3_9_,_1 FP_v
13)QS = (V) x US') 13) 9.2.Q.3. ACF_n
= (QS) x (Fฃ>/4) 14)__8_9.6_1. C^g
'= (tJO) x ( 530*ฃS. ) x (PSr29.92) 15) 8.0.4.1 SCFll
( ( S\ (~\ A O R "7 v I//"1 v *V* Q "\ J- /" Z^ny '/""V v T//-f 'Pi'f ^ ^ l' 'T'7"/f P v 77 v PC* y /I /./ ^ *1 c ^ Q P li "'
^ \UซUUiO/'^rL''^J^yT^ i w"- J O " r /*J T jt IJ / / ~ \ J. J. I- LJ "^ U ** Jt O * t\ H J J. D / -5 O*j_ f ป,ป ^_~ซ_.
= ( 15.43x^ ) f (VsrpD) ~ ~UiiITS : GRAIL'S/SCF
18)ฃ,'12 = ( 12xi7Si'P ) * (ฃ6'02) UNITS : GRAINS/SCF
19)ฃ50 = ( i'S2'px(100+/:/l) ) v (150) UNITS : GRAINS/SCF
- (0. 00857)x(gSinP)x(gsyP7J) UNITS : POUNDS/HOUR
"P4ซ2'JC;I/I/il'I'~Ii4B~^A^IysIs7o7
-------
HiiVlE.OLUllU.2AL EgGlUE EQLilS , LiiCQR
PLANT- CARGILL SIOUX CITY, IOWA DATE- 6/23/72
STACK- COLUMN COOLER OUTLET . Riff! 3 FROM 11-11-14-06
WEATHER CONDITIONS- CLEAR AND COLD P7?- 28.8 177 HG. PS- 28.'8 J77 l!G
AS'- "4.35 SQ. FEET TS- 574.7 DEGREES R . TM- 546.1 DEGREES R 77- 0.71 III' R^O
AT/- 1.07 177 7720 AN- 0.000341 SQ. FEET ' CP- 0.83 .VM- 86 51 CF VC-<03 ML
.TOTAL TIME- 110 Mil! NPTS- 44 OR SAT: /1//Z
"I')V'UV"To. 0474")*T'i'c')~
* (VT) t)~ฃ^03f)"" I~I~i
5)Fฃ/i = (1.0 - V) 5) ฃi.ElE .
6)ASSUMED MOISTURE FRACTIOii : e)..0.^0.!!, _
7}!W = (.44x002) t (.32x02) + ( . 28x (CO + 112 } } , . 7)__|0^5 -
9)CS = (MS} * (28.99) . ' 9)IIฐ[Sr
10)^^ = (100)x(Q2-0.5xCQ)T( (p.. 266x7/2)-(02-0.
n)/ii^c;(/(//>
-------
ENGINEERLUG, LRCQRPQRATEQ
UC CALCULATLQUS
PLANT- CAR GILL SIOUX CITY, IOWA
STACK- PAN COOLER INLET
WEATHER CONDITIONS- CLEAR AND COOL
AS'- 3.69 SQ. FEET TS- 555.9 DEGREES
42- 3.04 II! 1120 AN-~V. 000341 SO. FEET
TOTAL TIME- 120 Mill NPTS- 24 ORSAT:
DATE- 6/21/72
RV11 1 FROM 6:50-9:10
PB- 28.78 If! HG PS- 29 It! HG
TM- 531.1 DEGREES R 77-0.905 777
CP- 0.83 VM- 110.191 CF VC-66
= (0.
2)VSTPD- ( ( 530)x( WOx(p# + (ฃ#*13. 6) ) )*-( 29.. 9-2-xTfif ) 2). lL'i^.12. ฃฃฃ
(KSTPD) 3) L^ฃ-_ ฃCF
= (1.0 - V) 5 )~0^1-IIIIIHII
&) ASSUMED MOISTURE FRACTION 6) O^O^G.
7)/VD = (,44xC02) + (.32x02) + ( . 28x (CO + IJ2 ) ) 7) 2.8_U8_5_
8)W6' = (MD*FDA) 1- (18xp/) 8) 28_._5_6_
9)C5 =(WS)*(28.99) 9) 0.99.
= (100)x(02-0.5xCO)ป(-(0.266x//2)-(02-0.5xCQ) ) 10) M_ฃ\. . 2
' (tfxi'S) ) = ( 14//) xg {/.'./( J (H'xTS ) ) . 11) 21_._3_3_5 ..
12)i/ = .( 174xCPx(|/(29.92TP6-xG5) )*AVG( V(7/xT5) ) 12) 31.5.3.^.1. ฃPAf'
13)C5 = (i/) x (/i5'> 13)__il.(115.
x (FDA). . 14) UL-iM.
x (P5v29.92) 15)__1.0_4_5_7_
17)ES'J.'P - ( 15.43xJ ) i (VSTPD) ~UUITS : GRAIiislsCF "'
18)K12 = ( 12xSSTP ) * (/ป6'02) UNITS : GRAIIIS/SCF
19)ฃ50 ='( fi'Si'pxdOO+S/l) ) v (150) '-.-UNITS : GRAINS/SCF
2V)EM = (0. 00857) x(ฃ'5TP)x(CSTP5) UNITS : POUNDS/HOUR
~ "PARTicULATt:' LAB AKALฅsis(Gi4)~\ PARTICULATE CONCENTRATIOUS(GR/SCF) \ EMISSION
. i._y_j. l ISS^pj . IS.12.1 i^soj J .i.2
. FRONT HALF . - 11.0507 1.4914 133.65
B^Ctf 7MLF - .0039 .0005 0*05
TOTALS - 11.0546 1.4919 133*.69
1 ; ._i_
^ /#. . -U-
CQttl
-------
ERGlUEERIliG, INCORPORATED
!3k'ฃ S-AVPLIiiG CALCULATiQUS.
PLANT- CARGILL SIOUX CITY, IOWA DATE- 6/22/72
'STACK- PAN COOLER INLET . RUV 2 FROM 8:45-11:05
WEATHER CONDITIONS- CLEAR. AND COLD PP,- 2(3.9 IN I1G PS- 29 1 TN JIG
AS'- 3.69 SO. FEET . TS- 550 DEGREES R .TM- 529.6 DEGREES R 77- 1. 095' I.'/ 7720
ATj- 4:. 5T 177 7720 477- 0.0.00341 S.Q. FtfZ?!7 ' CP- 0.83 W- 144.691 0*1 VC-S2. ML
TOTAL TIME- 120 MI 77. 77P?5- 24 OR SAT-. ////ฃ
(b30)x( W/)x(pB-f-(A^f 13.6) ). )T( 29.92x2'^ ) 2) ilii^-JiM S0F.
= (IWV) + (VSTPD) ' '
- (VUV) i (KT)
= (1.0 - f/) 5) CK973__
ASSUMED MOISTURE FRACTIOil 6) 0^.02ง__
7)/./7J = (.44x002) + (.32x02) + (. 28x (00 + 7/2 )) 7) 2ง._85__
= (.MDx-FDA) + (18x{/) . 8) 2ง.iง.ง
= (MS) T (28.99) ' 9)__!li2^__.
= (100)x(Q2-0.5xCO)T.((0.266x7/2)-(02-0.5xCQ) ) 10) _MS
11) 25._675_
12 ) lZ[Iง.i.l
x i/io'J 13) 132Z?.I!
( PS T 2 9. 92) 15)1|ZEฐ IIiฃฃLf?
(0.
17)i'6'yp = ( 15.43xy )* (VSTPD) UfJITS : GRAIIJS/SCF
18)i;i2 = ( l^xi-oTP ) v (5002) UNITS : GRAI11S/SCF
19)ฃ'50 = ( fi'Srpx(100+ฃVl) ) T (150) UNITS : GRAIUS/SCF
20)EM = (U.QQ8$7)x(ESTP')x(QSTPD) UNITS : POU11DS/HOUR
~~PART~ICJLATe; LAB Ai\ALySI~slGM"\ P~ARTI~CULATE COlicENTRA'TIOils'lGR /SCF3 \ EMISSION
1_I_1_ 1 LKSTPJ. L3.121.
FRONT HALF - 20.8480 2.2737 ' 24B 44
BACK HALF - ' .0064 ' .0007 o'o8
TOTALS - 20.8544 2.2743 248^52
L / //i -, ' i'
COliMEUTS i _<^L&_ฃ: ^ฃj^__^__/_jCc^^7J!?S-X^l44 ^^T^d=Zl-J!.
i'ii'Si' CONDUCTED By : . - .__
(&& ) fni'irttnmenlal engineering, int:
-------
MVlRQ.UUZR.ZaL ERG.mEEB.lllG, LKQQRPQRAIEU
. ' SOURCE SAUPLIUC CALCULASIQUS
PLANT- CARGILL SIOUX CITY, IOVA DATE- 6/22/72
STACK- PAN COOLER IllLET RUJ1 3 FROM 12:30-14:35
WEATHER COVDITIOVS- CLEAR AND COLD PB- 28.91 If} HG PS- 29 1 177 HG
AS<- 3.69 SO.. FEET TS- 559.3 DEGREES R TH- 535.9 DEGREES R Jj_- 1.066 III'H20
Atf- 4.32 IP H20 AN- 0.000341 SQ. FEET ..CP~ 0.03 VM- 142.783 CF VC-S& ML
TOTAL TIME- 120 74177 NPTS- 24 OR SAT'. HI ฃ
_______________ _- 2SL. ~SCF.
= (wy) + (VSTPD) ~ 3)I_._4:^?_^I~icฃ^
6)ASSU!lb'D MOISTURE FRACTIOil . 6 )I_nIo.zaIIIIIIII.
= (.44xC02) + (.32x02) t ( . 28x ( CO + IJ2 ) ) 7) 2E.4.S.S.
= (MS) * (28.99) 9) IU9-9--
= (100)x(Q2-0. 5xCQ)v( (0. 266x/72)-(02-0. 5xCO) ) 10) M_5__ 3
< (/i5 ' ) 13 )
x (.FDA) 14)_.
15>ฃSi'PZ?= (WO) x ( 530Tin5 ) x ('PS*29.9'2J 15)Z
17)ci'rp = ( 15.43xy ) v IVSTPD) ~ ~UliITS : GRAIlislsCF
18)K12 = ( 12x_'Si1P ) v (%6'02) UNITS : GRAINS/SCF
19)ฃ'50 = ( ฃ55'px(100+Z7yl) ) * (150) y7/J?5 : GRAIliS/SCF
20)EM - (O.OQ8ST)x(ESTP)x(QSTPD) UNITS' : POUNDS/HOUR
"IfiuwJliTLl^'ljl^ I
FRONT HALF '-. ' 20.5451 2.2979 242 35
BACK HALF - ' .0095 .0011 : o'll
TOTALS - 20.5546 2.2990 242J47
.1 1
comeuvs : j^_^^..J^Jl&l,J^^.J^^^^^^^^^--^^2^^2:^
C'OtlDUCTED By : . ,
-------
MVIRQ.tiUMT.dL MS
, LILCQRZQRAT.EU.
LC CALCVLATIQU.S
PLANT- CARGILL SIOUX CITY, JOVA
STACK- PAN COOLER OUTLET
HEATHER CONDITIONS- CLEAR AND COOL
AS'- 9.51 SQ. FEET T$- 548.7 DEGREES R
Aff- 0.73 III 7720 AN- 0.000341 SQ. FEET
TOTAL TIME- 117.5 MIN NPTS- 47 OR SAT'.
DATE- 6/21/72
PUN 1 FROM 18:50-21:11
-PB- 28.78 J/7 HG- PS- 28.78 J/7 HG
TM- 538.6 DEGREES R ft- 0.447 IN 7720
CP- 0.03 VM- 62.065 CF VC- Zฃ ML
DVWV = (0. 0474)x( VC)
= ( (b30)x(KW)
= OiVlO + (VST
= (VWV) * (VT)
2 )__
3) ___ ^K
SCF.
( . 28x ( CO + 112 ) )
5)FDA ' = (1.0 - (/)
6)ASSUMt!D MOISTURE FRACTIOii
'1)MD = (.44xC02) t (.32x02)
= (MD*FDA) + (18xf/)
= (MS) r (28.99)
= (100)x(Q2-0. 5xCQ)r.( (0^266x7/2)- (02 -
9)G5
10)ฃ/1
______
8 )__2JLJL3_
9 ) 0 99 _
"
174xt72'x(|/(29.
11 )__1_Q_Jntal engineering, iru:
-------
S.U.y.rdQ.uMllU.UL E_u.aLiiฃmLEG, ILCQRPQRAT.EP.
' dQURCL SAHPLIUG CALCULATIQUS
PLANT- CARGILL SIOUX CITY, IOWA DATE- 6/S2/72
STACK- PAN COOLER OUTLET - PUN 2 FROM 8:45-11:05
WEATHER COUDITIOns- CLEAR PR- 28.91 IN HG PS~ 28.91 III HC,
AS'- 9.51 SQ. FEET TS- 549.1 DEGREES R TH- 533.7 DEGREES R H- 0.545 jtf 7/20
AS- 1.15 IN H20 AW- 0.000341 SQ. FEET CP~ 0.83 VM- 77.225 CF VC- 33 ML
TOTAL TIME- 120 MIfl NPTS-'HS ORSAT: /?/ฃ '
"l)V~kiv "To7o474lx'( ~VC) ~ ~ ll.
3)VT = (VWV) + (VSTPD) 3)___Jiฃ2 SCF_
4)y = (vwv) * (VT) 4) II^D^J. .
S)FDA - (1.0 - f/) 5) ^SJZJ
ง)ASSUMED MOISTURE FRACTIOii . 6) .D..^
7)//0 = (.44xC02) + (.32x02) t ( . 28x (CO + /V2 ) )
= (MS) T (28.99) ' 9)__J
^JJ.OO)x (02-0.5x(7Q)T( (0. 266x/;2 )-(62-0. SxCO) ) 10) i2SJCS *
H)__12..:Zฃ<
12 ) iฃI32*l
/151) 13) 1294H.
(FDA) . 14) 12Ji2a ฃ.PJ1D_
( 530 *^S ) x (PSv29.92) 15 )I_1ฃ32^II ฃฃ?ฃ/ฃ
n)3S'J.'P = ( 15.43xy ) v IVi'rpO) ~ "UUITS : GRAIUS~/SCF .
18)i,'12 = ( 12XESTP ) v U6'02) i///I2'5 : GRAINS/SCF
19)L'50 = ( fl?Srpx(100+ฃVi) ) v (150) WITS : GRAIliS/SCF
20)EM = (O.OOBb7)x(t;STP)x(QSTPD') UNITS : POUNDS/HOUR
p2Jf?JCi/I]l2'I1~H8~H'ZIy5l5TGiw')T~P^52;ICi/L3rS liblicEllTRliTWUS~('GR~/~s'cF] I Etil'ssio't! RA^E
FRONT HALF - .7494 ' ,1556 . . 21 86
B/1CA' ff^tLF - ' .0347 ^0072 1*01
TOTALS - ' .7841 ' .1628 22! 87
!_. ; 1
COiJDUCTZD-BX : .
~ ~" ~~ \v^V^ ) I'ai'irtntmcnlal engineering, I'IM*.
-------
lUdUtiUL MLLlilKmillG, INCORPORATED.
CE SAMPLILC CALCULATIONS
PLANT- CARGILL SIOUX CITY, IOWA DATE- 6/22/72
STACK- PAN COOLER OUTLET ' RUI-! 3 FROM 12:32-14-40
HEATHER CONDITIONS- CLEAR . . PS- 28.91 IN HG- PS- 28 91 If! HG
AS'- 9.51 SQ. FEET TS- 557.2 DEGREES R TM- 543.5 DEGREES R g- 0.552 Iff 7/20
Ag- 1.17 IN J110 AN- 0.000341 SQ* FEET CP- 0.83 VM- 78.785 CF VC-~3<ฃ ML
TOTAL TIME- 120 Mill UPTS- 48 OPS AT: /?//? .
= To. 0474Tx"( VC~) 1).
3= ( ( b30)x( VM)x(PB + ( AgrlS . 6) ) ) *( 29.92x2W ) 2).
= (VWV) + (VSTPD) 3).
= (Vf/K) + (VD 4).
= (1.0 - Jv') 5).
MOISTURE FRACTION 6 )__O^Q2.
7)//D = (.44xC02) + (.32x02) + ( . 28x (CO + N2 ) ) 7) 28.*.8.5
9)GS = (MS) T (28.99) 9) 0 99
^ (100)x(Q2-0.'5xCO)T( (0.266x/;2)-(02-Q.5xCQ) ) 10) |lฑi 2
11) 13^02.2. .
13)C5 = (H) x (AS*) ' ' 13)~ฃ83rLlIIZS?5"
14) QD = (QS) x (FDA) 14) 112.2.1: GKU.D.
x . (P5*29.92) 15) 15.4.11 SCP^
n)ES'j.'P = ( 15.43xJ ) v (VSTPD) ~UNITS : GRAIUS~/SCF
18)2i'12 = ( HxESfP') * (%C02) UNITS : GRAIliS/SCF
19)ฃ'50 = ( i'55'px(lOO+ir/'l) ) v (150) -UNITS : GRAIUS/SCF
20)Et-l '. = (0.00&57)x(ฃSTP')x(QSTPD) UNITS : POUNDS/HOUR
I'ARTICul^iJ^lAB'TiMllis^ ~\~EJil'ssJo7i ~Rfi^TE~
L_i_l 1 LE.STP}_
FRONT HALF - .3185 ' .0660 9 32
BACK PALF - - ..0138 .0029 0'40
TOTALS - ' .3323 .0689 9[72
^=C% (?...
COMl'iLtiTS :
Tij'ST C
. . <-s
-//
_ /s-'J^
pni'ininmt-ntal feaainefrina. inc.
-------
APPENDIX B
Plant Operating Data
-------
A. Process Description:
The following materials are blended in specific formulas to produce
a variety of animal and poultry feeds:
pulverized corn and milo
wheat middlings
soybean meal
cotton seed meal
fish meal
feather meal
meat scraps
molasses
premixes, minerals and drugs
Corn or milo is fed by gravity to a Prator hammermill. The 'mill forces
6 tons of corn per hour through 7/64" diameter perforations. The pul-
verized corn is boosted to the third floor by a 50 HP far. A cyclone
separates the corn from the air stream and drops it into one of two
2,000 cu. ft. storage bins (#5 and #6). At least 50% of the cyclone
exhaust air is returned to the throat of the hammermill, (see Fig. 1).
The mixed feed formula is placed in holding bins which feed it into the
California Pellet Mills. Steam is introduced to the feed material at
the pellet mill and the material is extruded through a die to form pellets
approximately 3/16" diameter and %" long. Each pellet mill produces 6
to 10 tons of feed per hour. The rate of production depends upon the
formula of the feed being processed. Fine, calcium carbonate dust may
be applied to the pellets as they drop from the pellet mills into the
pellet coolers. Dust is applied to feeds which cause problems by clog-
ging equipment or bridging in storage bins. These problems are related
to the ingredients in the feed. The calcium carbonate will pass a 200
mesh sieve and has been died yellow. It is applied at the rate of 30#
per ton of feed.
The pellets are cooled in either a column or moving pan type pellet
cooler. The rate of pellet flow through the coolers is dependent upon
the production rate at the pellet mills. The pellet coolers are located
in the basement area. Air is pulled into the coolers from the basement.
Dust picked up from the pellet stream is collected in large diameter
cyclones located on the third and fourth floors. The dust collected in
the cyclones is returned to the pellet mills for reforming.
B. Discussion of Test:
It was originally planned to sample emissions from the pulverized corn
storage bin vent. After the rain cap was removed from the vent, it was
determined that there is no measurable air flow out of the vent. The
calculated velocity of air displaced out the vent by the inflowing corn
is 0.1 fps. Meaningful results would not be attained by pulling air and
dust up the vent pipe at a rate greater than the natural draft, therefore,
the test was cancelled.
-------
Hammermi11
The hammermill was grinding #2 yellow corn which by National Grain
Standards, contains <_ 5% foreign matter and
-------
The first of three test runs was made on June 21, 1972, from 6:50 p.m.
- 9:10 p.m. A 21 ton mixture of beef cattle feed containing the fol-
lowing ingredients was prepared for pelletizing during the test period.
32% wheat middlings
30% cottonseed meal
17% soybean meal
5% molasses
16% minerals and premi
100%
xes
The feed was pelletized in 160 minutes, giving a production rate of 7.6
tons of pellets/hour. The pellets were dusted with 550 Ib. calcium
carbonate applied at a steady rate. Visible emissions fluctuated from
15%-50% opacity.
The second test run was made on June 22, 1972, from 8:45 a.m. to 11:05
a.m. An 18 ton mixture of beef cattle feed of the same formula used
for run #1 was prepared for pelletizing during the test period. Pellets
were produced at the rate of 6.1 tons/hour during the operating time.
The pellets were dusted with 500 Ib. of calcium carbonate. A grab sample
was taken of the dust collected by the cyclone. Visible emissions fluc-
tuated from 15% opacity to 50% opacity during the test. The visible
emissions were due to the pellet dusting operation.
The third test run was made on June 22, 1972, from 12:32 p.m. to 2:40
p.m. An 18 ton mixture of cattle feed containing the following ingre-
dients was prepared for pelletizing during the test period.
60.0% pulverized corn .
25.0% wheat middlings
9.5% soybean meal
1.5% cottonseed meal
_4.0% minerals and premixes
100.0%
The pellet mill was run at a steady rate, producing 9 tons of pellets/
hour. The pellets were not dusted.
The stack was observed from a distance of 20 ft. and no visible emissions
were seen. The stack was also observed from the ground level 150 ft.
below and 150 ft. east. With blue sky as the background the plume ap-
peared to have a constant 5% opacity.
Column Cooler
Pellet mill #1 is served by two verticle column type pellet coolers and
two cyclones. Only one of the coolers was used during the test period.
The column cooler was manufactured by the California Pellet Mill Company,
Model No. 2GA3, Serial No. 203664-2. It has a rated capacity of 7% tons/
hour. A CPM size 40 fan pulls air from the basement area (75ฐF) through
the cooler. The fan is capable of pulling 9325 cfm. with a static pressure
of 6" water at 1765 rpm. The cooling air and dust are blown through a 17"
diameter duct to the cyclone collector on the third floor. The 10" diameter
opening at the bottom of the cyclone does not have an air lock and the col-
lected dust is returned to the pellet mill on the first floor. The 30"
-------
diameter outlet pipe extends 27" above the roof. The cyclone inlet
and outlet were tested simultaneously using EPA method #5 with impingers.
The rain cap was removed from the cyclone outlet and an extension and
straightening vane was installed.
The first of three test runs was made on June 22, 1972, from 5:20 p.m.
to 7:45 p.m. A 30 ton mixture of poultry feed containing the following
ingredients was prepared for pelletizing during the test period.
75.0$ pulverized corn
15.0% soybean meal
2.8% wheat middlings
2.5% meat scrap
1.9% feather meal .
3^8$ minerals and premixes
lOOTOlT
The pellet mill was processing a similar poultry feed when testing began
at 5:20 p.m. The mill was stopped at 5:35 p.m. and restarted again at
5:50 p.m. and operated until 9:30 p.m. Pellets were produced at the
rate of 8 tons/hour. Dust was not applied to these pel letss and there
were no visible emissions from the cyclone.
The second test run was made on June 23, 1972, from 7:50 a.m. to 9:45
a.m. An 18 ton mixture of poultry feed containing the following ingre-
dients was prepared for pelletizing during the test period.
57.5$ soybean meal . ,
10.5$ wheat middlings
10.0% meat scrap
7.0$ feather meal
15.0% minerals and premixes
100.0$
The pellet mill was run at a steady rate, producing 6.7 tons of pellets
per hour. The pellets were not dusted and there were no visible emissions
from the cyclone.
The third test run was made on June 23, 1972, from 11:11 a.m. until
2:06 p.m. Testing was discontinued between 12:00 noon and 1:00 p.m.
A 30 ton mixture of poultry feed containing the following ingredients
was prepared for pelletizing during the test period.
18.75% soybean meal
3.50$ wheat middlings
65.00$ pulverized corn
3.25$ meat scrap
2.25$ feather meal
7.25% minerals and premixes
100.0$
The pellet mill produced 7.6 tons of pellets per hour during the 3.92
hours of operation. The pellets were not dusted and t^ere were no
visible emissions from the cyclone.
-------
C. Process Data:
Test Run
1
2
3
HAMMERMILL CYCLONE
Grinding Rate Material
6 T/hr
6 T/hr
6 T/hr
#2 Yellow Corn
#2 Yellow Corn
#2 Yellow Corn
Remarks
No Visible
Emissions
Test Run
PAN COOLER CYCLONE
Pellet Production
Rate
Dusting
Visible Emissions
1
2
3
7.6 T/hr
6.1 T/hr
9.0 T/hr
26.2 #/T
27.8 #/T
None
15%- 50%
15%- 50%
None
Test Run
1
2
3
COLUMN COOLER CYCLONE
Dusting
Pellet Production
Rate
8.0 T/hr
6.7 T/hr
7.6 T/hr
None
None
None
Remarks
No Visible
Emissions
-------
(vte>t>Eu G o^ -
-------
!? 'ft
PC I txiT
ฑฑ7
trp>
,\
. /'
~T
C. v"
V C U o r-i tu. *c-,-.'.'
fc l'l *' I .in .-^ ........^ ... J.-^.^.. .
CAI !'!".':'. viJ A rr. u'-r.v M/'-1- C'>.
).;,-, ic I ;'r, ; : V/^U '.-v._k.'_'-_'V COO U. ':.'''.
.
lii.'V v, -.>.?<:ป c.. c, en., i v : iS
-------
R.6.TU5N TO
MILL
r-
, - -r'r
- JO
MILL
ui1..
PSLLEir
COOLC.K.
Motsv:.L. Z GA'5
4n.'i;{Ai. NO. aosCiio^
- ;~ ~~^;~"'~ ""' "l J
CO.
-------
APPENDIX C
Field Data Sheets
-------
..
bainesville, t-loriua
SOURCE SAMPLING FIELD DATA SHEET
Plant ( i,
Sampling Loc
'Date /C~ 'J
Time Start
Sampling. Tin
DB ;^'/ ฐF..
^'Moisture^.J
/ .; ' ' ,-v... '- ,:.-.
.ation '.'/ ." -.'.''. , '
n - "/'s Run No. /
',* O 'AO Time End ^"-AO^,.S
ic/Point ^.b^tV'4 '' " "^j*ฎ''*
WB 71 ฐF, VP S DP (9. 67 "Hg
%,FDA c/
Sample Box No. | Meter Box No.___/
Meter ฃH@ / "'.' Pitot Corr. Factor J ,'J
- s /
Nozzle Dia.-X/ in.. Probe Length 6 ft
Probe Heater Setting
Stack Dimen.
Port and
Traverse
Point No.
| \J V^
A
1 "2"
| 5
! T
1 v.5*
1 d -
! jf-
i _ .,.-ฃ:i!
L jt
5ions. Inside
Inside
Height
ฃ?"ฃ>, J
Distance
from Had
o-5-Port
(in.)
^A**Tr^*/ ^^ tf **&&J^'
1 ^.* V . ^ ^*
|v-7v
/?'.-
i.y^a.
|9&t'iป ^ >__ . ^
3/'/;
_ .
Diameter ^2 "/<* in
Area J4^P
r'"'>
d^aT '/2^ /,^"
^o75ฐ /ซ4^ /4^
^,o<^ /-v^ A^T-O
O.. ^J /ป5& /<5b
_
_L^gZZ2Z:M2
v^^.-^"
, . ,.,
Stack Gas
Temp .
CฐF)
^l
j^ " *
f*~- * ?
*r*w^>ป F
fc -*^*),, ./If-
*ป.
n
--
C5b^ i /-4Ta /^5bj *-
>r,.~ f /'.
./ . ^ --->"' ' '-' /
*&**" -- ""
^~"
v _ / j liiL-i^^:; ;_..__,
Temp.fJ Dry
Gas Meter
(ฐIO
In
7?
a* -<
fif*' r '
73
72
71
7t
7a
Out
_7^-
'"*( ซ(H
7^-.
7^.
77-
72.
7*-
,- -i
||
L,^t>
,"''
7-5*
/M
J2ป5"
J_So
1-6^
Last '
Tmpirgcr
Test
-.. ..._..
^ J
.
^.
-
Yacu-u;]
on 1
Sample
Train
C'Hg)
7- ^'
* ^*ซซRป
s-^5"
3^5*
2 <-
S>"ปซcซ>
v-2-vT
. 1
-------
Port and
Traverse
Point No,
/.V?'V
Distance
from End
of Port
(in)
A ,-. / !i-
/? -.-. ~J <*> O-''"j^2.
f ' Ci //fc
>.: 7 (.%_
Clock
Time
T;t-%
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Reading
(ft3)
; ซซ. _
7^7/7
_/?/'
/72.7
. ป,^-
/ 7 '/* ^
Stack
Velocity
Head
("H20)
^. 0%
o,o7
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p,c>7
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Press, Diff ป
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Actual
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Temp.
CฐF)
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.
X<5 /.G/J ^?
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0-30
//* \ f**t
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77
7/
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-------
Port and
[Traverse
ipoint N'
id Distance
;e from .End
Sto. of Port
vC fin)
-y* t,w>flฃ [
' '1 '
A **** )* .*
W' ; ***** ""' I '->
i^5> J ,/ J-"''T"ฃ
'7: ij-i-
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Clock
Time
ซ; .
&A }'"*? ซsf*
_|O f' l*3$>
' ^ Ifty & l^1^
! B "fcf felfeS'
r/tfti^-
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Gas Meter
Reading
(ft3)
j;r;v(
i v. , -^ -'
! -) ,7 t ^
f / ' *~ '
I I ;-^,;^ ,:^
Stack
Velocity
Head
("H20)
' .O
ฃXv-.}.:' '
0, ()J O
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' ) "' '' 1 tlZ1.-
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Meter
Orifice
Press -.r/iff,
!"H20)
.Gale, j Actual
1 "" ^f. ," I u
/"/ ' : ''i - ""> ' '' "i
Of?o\o."-J0.
0 J-ft OoV.O
j 'ซ> ,-v s . .,, -^.N
O 8 ''.''- ! ''.'>:>'.'."'
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Temp .
CฐF)
ซ-
Ha^ '
i ,.... ' %.,.,]
^' ^
1 o <
1 .' -'
Gas Sample
Temp (ง Dry
Gas Meter
Tn Onl"
.
ป ซ,
/.'/( (",'
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6>' ^4
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BOX
Temp-
.^ซ=-
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Last
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Temp.
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1
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Sample
Train
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,
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tj'ort ^7]
n raver z<ฐ
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jCk
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from End
of Port
(in)
Clock
Time
Gas Meter
Reading
(ft3)"
j /<>- /
~ *5 f> ป f
ll/y \lllM
_ ._. j a.^. -. _
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T /?:
Stack
Velocity
Mead
("H20)
O.//
Meter
Orifice
Press. Diff,
Calc.
Actual
Stack Gas
Temp .
c.
Gas SampleF Simple, j Lnst iVacuum
Temp.!? Dry-
Gas Meter
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.J-jpx" ) Jinpjngerj on
Temp iTemp,
an
Out j 'I'/.','-
iiTTJ"^
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Tป
f
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-------
Iport and ~] Distance
JT.avt^ic > from End
JPoint No. j of Port
Clock
Time .
Gas Meter
Reading
(ft3)
Stack
Velocity
Head
C'H20)
Meter
Orifice
Press. Diff,'
C'ii2o)
tack Gas
Tenm .
Gas Somp'lei Saiiip.lt; j Last j Vacuu;:
Teiup.@I.'Jry j BqS^'j Innp'jngerj on
Gas Meter j T^rnp,., i Temp.
Sample
Train
-------
ENVIRONMENTAL ENGINEERING, INC,
1 Ine: lie, trie )
SOURCE SAMPLING FIELD DATA SHEET
Plant f' " " ' <' :':" <'">'
Sampling Location ., %'>.' , ,/*.''-ฃ
Date . ' ' Run No. S*
'",."- .-- Mat'l Processing Rate
-ซป
:Time Start / -> .' /Y) Time End //-":
Sampling Time /Point '",,C>( ior^/z^^^-^
DB ฐF, WB ฐF, VF 8 .DP
Mo 1 s ture 2,31, FDA ' ~ , Gas Density F act or
Barometric Press '"'.V'.'Hg, Stack PressZฃ7
Weather
Temp. - ฐF, W/D ' ,W/S r- '"
Sample Box No.. / Meter Box No. /
Meter AH9 /ป""/ Pitot Corr. Factor . f~?/
/
Nozzle Dia. / "' in. , Probe Length (~>
..',-^75
"Hg
ซ- *
ฃ'Hg
<- '.^
6 .:>
ft
Probe Heater Setting "
">, f ~* *
Stack Dimensions: Inside Diameter
Inside Area '/. . '/(*
Height /,
in
tt2
ft
,ฃ M^, '
Final Gas Meter Reading 32 "^. 3 ฃ ;y ft3
Initial Gas Meter Reading ; > "7*7- -2^7^ ft3
Total Condensate in Impingers / V ml
Moisture in Silica Gel -~._ gm
Silica Gel Container No. .- Filter No.C":" ' '
Orsat: CO?
02
CO
N7
Excess
Air
Test Conducted by: /\- ฃ){j / :'<' tf/S
r > n^"---/'
Remarks : [^
Port and
Traverse
Point No. '
>S-H
, - ' ' I
1.
'
! .
t
l-
Distance
from End
of Port
(in.)
* > * '
,><,ซ -
* f- .'
/';-.:-
!
/
ff
1 .'
Clock
Time
/ r.^
!?./?.$ป
/U$
t
1 ' ; 4,
_ , ..' 1 '-'
i , t .
^
Gas Meter
Reading
(ft3)
Z.77.-270
rr.'V^
" }
^ - * ^
-. '' '17
:i ;"^:^
i
Stack
Velocity
Head
("H20)
0.fฃ
^,a^
o, --:
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" ^~1
.- ซ'V":
**\ '""-
*
Meter
Orifice
Press. Diff.
(""20)
Calc.
aw
beft
,0.f!--'
r . 97
/.?'
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$.
i t
Actual
/O ("> o
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/ . .
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Temp.
CฐF)
s~*f3
f-> /
' "?
Gas Sample
Temp. 9 Dry
Gas Meter
(ฐr;)
In
7/
71
** ~- '
s.
/x
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f f
'_
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tf
f,''?
i
i
69
{''I
\
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Box>
temp,
JฐF>
2r>
^^
/
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/
' -
Last
Impugcr
Test
(ฐF)
-
/TV
' i --
Vacuum
Oil
Sample
Train
("Hg)
Sf*
ffv
ป 1 ,
1 ,''''
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^ .
-------
'ort and
Traverse
Point No.
*. ' /
f . <
\
t i '
> \
T .
' .
-ป ,, . .' ; *
,/ / . . ' i '
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1 ป ;
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(in)
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**" * / .'
<! Yit.
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1 '''
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Clock
Time
1 2 - o
1 -^ - : '-
1 -'- '' ',.
/:: ; ": '
j i
) ... - .
' -
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./ ,v- -#"-."ป
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I ' :
!\^>-
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Gas Meter
Reading
(ฃt3)
^d*"^
0,-lj,y
XI 3* -1
^5? 'A "7
^J^o-
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/ " , ;' > ft !
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''.' J ' "'
. ฐsf ;' ! 'i
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.;:-,' "s-
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Velocity
Head
("1I20)
^ป Oฃ"
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r>. o.S
c^ป o,S
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11
=>l II -
. 0. /'/
ซ>, |'7
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Orifice
Press. Diff.
("IbO)
Calc. 1 Actual
r t;.^
1 ,' ^-J
1 > t.
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0-!^
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Stack Gas
Te'.np .
(ฐF)
"?r^
-
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^~-
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Ci'T^"
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f;?
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9
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Temp ,0 Dry
Gas Meter
TO
In
ซ-^ r*-
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- ; f '
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/
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"7 0
V1
''.--' - .'
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77
; ^ ^.
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^Bek--, j
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.eฐr)'
.y//1/
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t'-.f,
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Last 1
Lirpinger
Temp .
(ฐF)
ฃ'< i
,
Vacuum
en "
Sample
Train
y.o
' ,-
')
1
73 _?4/'
X
ป--. x
/->
i; i
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ซ-, /
v1' 7^
/ ' "^
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. . . /
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/
7 "7
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. ^.D
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7 -5
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''-.-3
' ' '" i
' . v '-,, |
/ ^ !
-------
Plant
ONMENTAL UNGINEt-RING, INC,
utAn.ei.vj.Jle, i ...iriaa '
SOURCE SAMPLING FIELD DATA SHEET
. . Mat'l Processing Rate
Sampling Location
Date
1 ' Run No.'
Tine Start . )"J ', s ' Time End
Sampling Time /Point
DB __ ฐF, WB _ ฐF, VF @ DP
Mo i s ture _ % , FDA_
Hg
, Gas Dejisity F act or
Barometric Press _ "Hg,- Stack Press_
l\'eather__
Temp . _
Meter Box No.
_ ฐF, W/D
Sa;np3e Box No.-
Meter AH@ Pitot Corr. Factor_
Nozzle Dia. in., Probe Length_
Probe Heater Setting
ft
Stack Dimensions: Inside Diameter_
Inside Area
Height
in
Tt2
" ft
Final Gas Meter Reading
Initial Gas Meter Reading
Total Condensate in Impingers_
Moisture in Silica Gel
ft.3
ml
gm
Silica Gel Container No.
Orsat: ' C02__
02
CO
N2
Filter No.
Excess
Air
Test Conducted by:
Remarks:
Port and
Traverse
Point No.
>
; '''. -
">'.-" i'
i
ซ*
r '
_
i
Distance
from End
of Port
(in.)
- v ^
: "; . .
T
f" ' "
X * *
j'-YiY;
Clock
Time
* "
/ %?'
\ ' ? AA
/;'"
/*->:,5
/:-'5
Gas Meter
Reading
(ft3)
v i r f
>J-/,q
^r/:>ป f
-?;, r.
v^r-rf-.-^
5 ?-*?.. ^ AT.
Stack
Velocity
Head
("H20)
o./V
1 ,J(
* 1
^ . i :>
0 ป / )
^ . H
or//
o.'//
Me
Ori
Pres
C"
Calc.
^,7-'-
?--.'
w ' -
3./:
m . ; .
^ . - ,*
^L/
ter
fice
s. Diff.
1-120)
Actual
^^ ***? v.
''"' *
*^ * *"
;> ..'r;
/ t / XJ)
;.- * / >
&* I
ฃuJ-
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Temp .
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q 2
. _
^
q-a.
.
Gas J
Temp
Gas f
(C3
In
79!
V
^ 7
..*" >
/ "
fa
Cample
@ Dry
leter
Out
O! ''
* >^
7ฃ
'/7
y 7
%--,'
* *' -i
1? ซ:
Sajnp're"
Bc.x>
ft '- i
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'- ,
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f.
jr^;
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Jr.ipirger
Test
,<: V
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.....
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-
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on
Sample
Train
("Hg)
// fr
'
-
V"*'
//./)
' / '-
7ซ .v>
-------
Gainesville, Florida
SOURCE SAMPLING FIELD DATA SHEET
Plant ".-* i ' : ' ,''.-
Mat'l Processing Rate
Sampling Location ฃ?-./. <-/.^sJ Ct/!''J/~_r//S<7~)
Date /^ /^ Z/T ^ Run No. /
Time Start / ',' 25" Time End M /Y
Sampling Time/Point /.-, ^/"" ' T"-" '
DB ฐF, WB : , ฐF, VF @ DP Q.8&
Mo i s ture^, 6 ""= , FDA , Gas Density F act or
Barometric Press'V- "Hg, Stack Press 29, 2
Weather ^ -
n
"Hg
"Hg
Temp, r/0 ฐF, W/D ,W/S
Sample Box No. --'; Meter Box No. ./>
Meter AH9 /' ' Pitot Corr. Factor ' " '"
Nozzle Dia. .'" "in., Probe Length >
ft
Prcbi Heater Setting
Stack Dimensions: Inside Diameter /^ -V-'
Inside Area
Height
in
t't^
ft
.:
^"' .' ,- ,
Final Gas Meter Reading ' ' ' - ' -:: O
Initial Gas Meter Reading /"" / - ' ft-5
Total Condensate in Impingers ฃ //'
Orsat: C0?
02
CO
N7
Excess
Air
Test Conducted by: /ฃ ^//rVy
.r n // . :
/
^~5
/ s*~ '
Remarks:-^- /-' /<>/// v> j^. .,- , J >' .
*
Port and
Traverse
Point No.
far /
M. /
/
k- I
a
3
3
Distance
from End
of Port
(in.)
/
Z/t
5
Clock
Time
/7/^r
/7;^
/7.'5r
/ (3 T; './
/ (J <~J <^
I '
i <:) , A
L,. ! ^
Gas Meter
Reading
(ft3)
/^'/~?
' 1%'
'& ,."
j' '".'
t
$ //- f
Stack Gas
Temp.
(ฐF)
/'/: /
* ' rf;'
i; 6
-
/ /<-
Gas Sample
Temp.i? Dry
Gas Meter
(ฐF)
In
:-"."
?/
h
/
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Out
.. .-'
eg
g&
"- f
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Sample
Box
Temp.
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ซ>ป*ซ'
.
~_
.
.
Last
Impure r
Test
(ฐF) .
12
7 &
r>' :.?
7Z
7f
7-1
Vacuum.
on
Sample
Train
("Hg)
t
" * i.-
:^^
? f
i. .*--
7 -'?
? ^>
*
* '
-------
Port and
Traverse
Point No.
//
u
4'
5
X
/
~C
,/.,. ; <ฃ
/
/
;:
X
W
-^--'
''-'
//
-
>v
'
*ฃ
Distance
from End
oฃ Port
(in)
.'/ '-' .>
11- -^
15 7/3
/
'} Vz
'ปป,
n '7/V
/ 1 f ' H-
' :' > V "
, f* -"': f
0 / S
Clock
Time
it
A?//7!
/ ';' '' r"ป ^ >
I } .> r*~. .- >
/#.'*?
t, ' ~ -\
' ' ~ , ซ*'.
18 0
- } '' ;:
; J '
tf; '''/v
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r?///
/ > : :"'.
/<9 / A 1
n;zฃ.
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/v,,;i
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/?;vr
6 '"-* ' ,*'' *
Gas Meter
Reading
(ft3)
.r -5\ -/
;<^,^
. , ,, * ,r-
" ^ -C'
3'-/<ฃ
""/' -V
t,- (y ' f
"1s . '" ' .-T*,'"'
/-~ A" D .
.-.-'^. /
// /- ^
.-'/'?. 2
-V^/' ^?
' * / / ,.'T-
* .' ^/
'/'ฃ?' ,'f
,r^- ^
,r7 :-f ^
,cr- 2.
^, -y
,^, r
/r/. f ^tf
ffW
Stack
Velocity
Head
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/
0 i
^- * V
/ J ',
/ . '. S-f
' * # C-'
/. v,.' ~5
/ ** ''./' ^--!
A Zo
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/ *" '
/. .'-" c"
/, ^"^
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2, /
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Meter
Orifice
Press, Diff,
("H20)
Calc.
ซ- * * ^
O' ' V0' \. '
/;. .'/'j
*> ? .-' *"
>
/ *
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# '
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<=< I
Cff
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r
^
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?<7
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CT f
Sample
Box
Temp.
TO
._
ซ-.,,.
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-
....
^-
^~
-~,
ซp(R.)
^>
._.
m.ซ
-*~-.t*.
^saop*
^.,
Last
Impinger
TeirtD.
(ฐF)
/?<
7O
6Y
cS?
^
on
Sample
Train
:':,O
J1, o
- **
^"j ^
.-< o
""'" . <""
^,r
tf''T rt
*.' //
\ ซ ""
V.o
?.t?
T''*- "'."*
^ -A
1; "7 ซ. '
(f ' *
- .- * *'' V
jC ^
-:-, 7
'>'" ; ""^
3-, <^
0^(3
...?, -c?
.}&
-------
liiNVlRONMliiNTAL UNG1NLT.U1NG. INC,
SOURCE SAMPLING FIELD DATA SHEET
Plant ฃ.
Initial Gas Meter Reading >J /, \0 .^ ft-
Total Condensate in Impingers (_
jyr- /o5"^- pjirfsi- V/O;3l so
Port and
Traverse
Point No.
tP*tTl
i
/
2
^
3
3
Distance
from End
of Port
(in.)
/
2ft
5
Clock
Time
'7/Cc.?
7.'Cr
;./,"'/
^J;/3
.?,'/*
?.S '."
Actual
-: ;r '" "
o.,4?"'^
<7-J^
'-.^'75'
o- '/-?
#.--/r
Stack Gas
Temp.
CฐF)
//2-
/ ^ 2-
//^
// z.
// z
:/J_
Gas Sample
Terii}^ . 9 Dry
Gas Meter
(ฐF)
In
??
?J
7^
73
7?
?J
Out
^V
?f
w
?f
7?
?y
Sample
Box
Temp .
(ฐF)
*"
Last
Impure r
Test
CฐF)
v-j
'] v'V
--r-^
/ ^
70.
6ft
To?
Vacuiun
on
Sample
Train
C'Hg)
n t o
*""- f~
*ซป '"'
ป v
^""
^,
2 .
-------
Gas Sample
Temp. 0 Dry
Gas Meter
Sample
Box
Temp.
Port and
Traverse
Point No,
Distance
from End
of Port
(in)
Clock
Time
Gas Meter
Reading
(ft3)
Stack
Velocity
Head
("H20)
Meter
Orifice
Press. Diff,
Calc. Actual
Stack Gas
Temp .
In
Out
Las t
linpinger
Temp .
Vacuum
en
Sample
Train
.5
s.
f
7 3
0.&
ซ?i
5
r?
5
"
-------
ENVIRONMENTAL ENGlNLKKiM*, IMC,
SOURCE SAMPLING FIELD DATA SHEET
Plant '
Sampling Location ^V; ////r// /> *(< / ~rt-.IJn
Date -x/: ' ' ': Run No. '-' .
Time Start
Time End
'Hg
Sampling Time/Point / "
DB ฐF, WB ฐF, VF @ DP
Mo i s tureg,,g"%, FDA , Gas Density F act or_
Barometric PressZ^'Hg, Stack Press tf.O "Hg
' Weather -" ' i '.
F, W/D_
,lv/S
Saiiiple Box No.._
Meter iH@.'
Meter Box No.
Pitot Corr. Factor
Nozzle Dia. in., Probe Length
Probe Heater Setting
ft
Stack Dimensions: Inside Diameter / > -'< in
Inside Area tt2
He i ght ft
Mat'l Processing Rate
Final Gas Meter Reading /-.^X ''_
Initial Gas Meter Reading / - ^_
ft->
Total Condensate in Impingers
Moisture in Silica Gel
ml
gm
Silica Gel Container No._
Orsat: C02
02
CO
Filter No. //
Excess
Air
Test Conducted by: ฃ-. /?/.'"/"
Remarks:
Port and
Traverse
Point No.
it i ,
tfTf |
I
/
3-
,2
?
?
Distance
from End
of Port
(in.)
/
i
z'fc
f
Clock
Time
ll;o o
ir.of-
\ttto
ir.i?
ttiw
i/tir
Gas Meter
Reading
(ft3)
'ttf. W%
I CO, u
/M,5/
//?- t
tiS.o
/Ai,f
!&**
. Stack
Velocity
Head
("H20)
LKo
f.tfO
1 , -1
l'&
f.&o
(,&>0
jrt*
Me
Ori
Pres
("
Calc.
/oy>
&?jff
tffvr
-l 5
. --
') ..-'' -
Stack Gas
Temp .
(ฐF)
.
// &
f/&
// %
^
t i -^
: / "
Gas Sample
Temp . 3 Dry
Gas Meter
(ฐF)
In
11
"7 F
7?
' j
; > ?
Out
-11
fl /
f7/
5/;
.--, .
Sample
Box
Temp.
TO
-
.^ -
...
,-~
Last
Impure r
Test
(ฐF)
y/r
.' '/
74
11
:,.'-
\racuuin
on
Sample
Train
("Hg)
* r'
;?. G-'
1-0
''-'. c~
-------
1'ort and
Traverse
Point No,
4-
tf
s1
s
6
&
/} -lป p"j
**!, Jfr T*ป Jf
\ d^ \ '-
v<-'f
' // ',"''.."
/-/ ""'-,"
/ ^-
Clock
Time
il;3ฐ
/i:3S
ll'> H*
1 /.' <6"
//.' Sฐ
//. ob
/ -
: -'''.^
/'/' /'-'
/ / .'
, '^;^
Gas Meter
Reading
(ft3)
. /i-v?
/ Z.5, /
/ , '*?'-'
/ Z 7, Z
/'.?.-'?* ^
. I ,..,-* i-7 '
1 ', ) J V <-' (*
/.,; .-,> s^,
'. . ' V-
., - : .-
/ ''"'' . /9
/ . ?,<": .^
/J?^'
r.--f,6
/>'//> #
A: /C '"/
l-'-iS,.6
/HI, 3
/ ' f: 0
if. n
/*:./, 1
if:i fi^ f ,
' /^ /(/ /
i^^^it* ^ \,P *^>15W
Stack
Velocity
Mead
C'H20)
'A y^1
?,/;/";
/, 7
.'" x ' ''
-?: . v?
/< c?o
A ^
A 7
1*00
1
Meter
Orifice
Press, Diff,
("!I20)
Calc.
3. t/i!'
ป ' . -}
f* \ ' * ,
t) S?f
-?.'. '.-' '"
O-c?75
': f: -
^.:'> 1 '>.
0. fv
. " - " . -t
-- ^
,.-; C'. r'
<3.57..*;
A*l ' / ' / '
f*-yV '' ' '
/' -f , i ^ .
' '. *"
^. ff- K
4> c(&
i '', '/
/ / 1 'i
f> , ' i~-
Actual
/
j , - : '-
.: '' . I"
. -f i t j * ^
* ' /
, 7 C7,"
<'-. .-,; ;','
'";. ,/ / "
^So
<. , ?'
.'}*<.' '
-: ''',' ' '}
A,t /''I""'
W ' ' ซ
<-, H1
.}>! t>
,-\ .
/V.'/T
/* g ; ff
('i ' .:
'; "; - '? '*
.^H't
Stack Gas
Temp .
(ฐF)
// g
//s
// %
//f
//,f
/ ''/ p
f / <9
^llA
'//&
#ฃ
//S
//&
//ฃ'
'M&-
//$
S/6
//&
'//^
Gas Sainnlcj
Temp. --Dry
Gas i-eter
(;'F)
' In
', V
/ /r;
,' i/'7
r/ n
i '
; '>
/ :">
f;i 0
i ; -
n '-'
' ','
??
n> '
#>
' /
.."?
'" ,'
f'} L
',' '-,
^
Out
'"' V
' .' ')
n "-
i
i ' "'
r> "-
' V.'
,->:-,
}
- : ' /
'' ': ' '
/' / ' ;
-? /-?
' /
r-| ...
/ //
' / "
' i *
' '' ^"
r/(:;7
/^
9"/
i
Sample
Box j
Temp -
(ฐF)
-
__.
W~1M,
..
^J.V.-,'..-.^
.
.
-
~"
.-
-
Las t
Iinj^ingcr
Temp .
(ฐF)
f .i
j"
7- '?
Vacuum ^
en
Sar.ple
Train
-^ n
-< > ^
7 ?, ' i.-;;^
70
'' / . .
" ,v
*-'* . ..
V '' t "
^- ' ..- t'X.-
.;: /
>ซ-*
..^jP-rorf?
^7
AOปI>* /
' 10
vซ,' ^ / ^ '*2$
/ - / L<. 5
)ซ..-ป
7 7X
7 ;f
Vv,J
rr-
/ .- .-
n -ฃ
S/
.:',//
_, -*.
. rf .>
^?./-
n, /
-------
^.VIRL^ JNTA_ JJGII IING, uc.
Gainesville, Florida
SOURCE SAMPLING FIELD DATA SHEET
ainpling Location
)ate -'.'
Run No.
ime Start
Time End 7/'/'-
ampling Time/Point f ' - - > - . .ซ
B/:-^- ฐF, TO ' ฐF, VF @ DP '^ /7/ .'/ "Hg
,Gas Density Factor
barometric PressQ' ' "Hg, Stack Press
Weather
iTenp,
:, W/
,W/S
ISainple Box No. / Meter Box No.___/_
Meter AHS '.' 'Pitot Corr. Factor O - X
Nozzle Dia. ' in., Probe Length
.Probe Heater Setting H__
ft
Stack Dimensions: Inside Diameter
Inside Area __/.V
Height J_
in
0--
J
i -'
Mat'l Processing Rate
Final Gas Meter Reading '>--. .''/'ป.. '
* ' . i * ? ?
Initial Gas Meter Reading xV '- _) / '/ ft-^
* -1* " t '
Total Condensate in Impingers '_/ / .rcl
Moisture in Silica Gel '~ gw
Silica Gel Container No.
Orsat: C02
02
CO
Filter No./
Excess
Air
Test Conducted by: /V,
Remarks:
ฃt
Port and
Traverse
Point No.
^> 1
t. u" ^ '
n.^M-/
1 2
3.
ฅ
5"j
.
Distance
from End
of Port
(in.)
i -,, ,11 j* i
V c -
i -
(;-
, !
Clock
Time
1
/
<;-;> <
.' ป*
>< . - *
:-. v?
\ ' . i
',- N
11
Gas Meter
Reading
(ft3)
o-v!
.- . - , i . |
-M/^,f f
';-;-.o
" ' ซ , ' ."'
t
r '/!-, -'
. - - . .1
Stack
Velocity
Head
("H20)
&t -^
S).<*
r^ t ' '
t * .
c- . 3/>
0,V':
i' .' ^
ซ
t
Meter
Orifice
Press. Diff.
C"H20)
Calc.
//:
ff
//
f t ^
; ,
I i ? i^
. ,
/ t
( !
)
Actual
./ ,*
/.-ซ ?
./,-
/t, x.
/,.'.
t r?ซ,
ซ * - "
1 ,
Stack Gas
Temp.
(ฐF)
sฑ&
/**:-
h^l
'/^
* . ป
** v l *
1 .
Gas Sainple
Temp.O Dry
Gas Meter
(ฐF)
In
ป^ -*- "*
-r
7"f
vV
x )- >
*- r
* " /
Out
* . ^
>ป * v '
ป * '
" ; '
< , /
}C
* ff'
/ T ป
Sarr.ple
Box"
Temp.
(ฐF)
*^: ^5
4 J *
,<,t>
7^"
/r,
; !
/'--
Last
Impirge r
Test
(ฐF)
/, -
* i
/ -*
ซ >
VuCUUIT;
on
Sample
Train
C'Hg)
f- * -**
**,.
I ,'---
//,/ '
//, '
< / /
-------
r
^ort and
traverse
Point No.
f
1
Distance
from End
of Port
(in)
'' '' -'
i
'.
L_ ' "
-'. - ".*
1 ,"..-" ;
" :
;<
j
'
', ป '
,
/ ' f
.. ' ' ' .'!
?
,. ' " '"
Z7 ซ'y?
?J7 "?ป?
;? - v- < i
'. * ' - .
Clock
Time
,ฐ >; ..
t > .!
. ! ' /*-".'
'. -; '' V '.I
* . '
4 . ' " "
>* ; !
fV /> i-..
C*7'',?:?
Gas Meter
Reading
(ft3)
"'/ ป T3
7'! *> /. ','
/w"-^'-, * * \
"'",S ., . . J;
"B7' q
/V'^'1/
v.; .sV'i V,'<ซ /
'' ' \
-, * | 7 -7
D * p.'"' "* ^
7''77
i ' :'3
- ' 2 v ;
ฃ/.ฃ0'
/,* /3r*?.i
^;=;-s
...
"-
/;^7'
7,"'7- ^
Stack
Velocity
Head
("H20)
' ^-, >'>'
C '" * - " * , *}
^,77
/ / *
f3, /"
^ ,Y" ^
f"'.!ป v'!/.
t-*7ซ:>
: r.\ 6;'>
oป ?:b
i% /-/.
d*,>o
("; ซ ,'"ป
c5>/ V.'^
/
jj?^ ' ^i
t$ -n 6 ' "s ^
rQr/Zฃ
& '
D
0;
(ff
U*\'
Meter
Orifice
Press, Diff,
("H20)
Calc.
/''/,;
/. O-/
A''',"
), /A
/! ซ.' i.-1
/ 7 ',
.>"" ^
" ' > .
,1 -? */''"'
1 ,N ;
.l:!i r'.1':
|,'70
/ ' / *
;}
/ , ,6r
J,r';:
3ฃ?~ฃ
^J
O
O
o
/""*
Cx
(-3 , -) '' ''
Actual
/ , . ; ,
/- >,
* ,:-
/if'*
A ^:?^
', ) . . i
r ^ . . ,
SL- * ป'-- '^
2 *^7'
A ^-o
Av'/
AX^
/ / ''' ,-".'
^7? ''
^p?;<
'y;z3?
o
fj
(^
1?
i..,' , / '
Stack Gas
Temp,
CฐF)
'/ /'.'
Yi'j
^/''j
u'1/
/n u
V<'';//
/;vJ
/?'*;/
/7t<
/o&
' ! o :
/i\ /-,
'/o ฃ
/*
, u 6
/7 {
' X^-<
-
1 0 L
Gas Sample
Temp. @ Dry
Gas Meter
In
7 ;, -
/ ~>
7-:
") V
/ "-
Out
Sample
"BOX---'
^Teirfp,
yyT^T
* . t
* ,! '' >
V/<
'/ - *
v, V.-;
" / 1;
v r
ซ /!
/''
*' /
"'-,,"-1
7' *>
7?~?
Ox
/ . ,'
7 7
7 ' '
I/ *v '
/ / ;
-\> '
' ' ' t"'
*7 X"
i
7*/ *
?S
.
*
^()
7* 5
/>.<:>
f- ,- ) ฅ. '
/.'''"
Last
Impinger
Tenp,
i
,.,-
67
..
. . . .
.,.-,-
r.'- ^:
|. K
77.^
/i?.^
.'" ซ- '""- "
*" ' '
- ; F
f, ,-.
v .r
//. 7
ฃ'~* -ป"'
jJv-^
-
... .1,
j --
7>-^:-:
-
>-
.ซ,.,,,
CS
s-.
. .
-,,,.
. -
,.
-
ซ..
t '..-'
Vacuum
on
Sample
Train
t > t :
'/' -
' '.
/' ''
V'V-
.* . /
' ,'. ' >
' '-.. ',
- c
' ,' :'
'/.:
^ .-:.
," "-.
";' *
(;v..^
^ ' ;* . *^-^
;---/,ซ./*'
-..
'' / - \
-------
:t and
.averse
Poin" No.
/X:^'9
' j /
' .;"'_' ' f'
Distance
from End
of Port
(in)
3;^
\< 71 4#,
?
ฐ\
lo
} i
I /::
- f!
j ''. : ;
5'v--:--'
Vy ^ . -
ฃ '"/< -'.'"
S^::,
~ -j ~* / f
*T. '} t -'"'" -o
Clock
Time
^;> ;r ,
ป'* . . - 1.
/ t <' '.>
' 'i ', "* -
- t "" ' I ?
V-/0
*'-' ',-. J-
i\3/Ll ' ".' "'
1 7 ?''*!
/<=}':? A- .
'' "** \'' >J i
f
1 /
' / "'
/''
i Pi
1 ' .
-""! i
-, -.
.,Vl
.
J ^-\ "I i '
;;>'..' \x^;'..
2V %
^ ^?
/r? t'';-
i,>ฐ ,* ป ?' ป
g,r7 ?:,ซ
\
'-* ', '?'
V ':> r>
V">"- f
'- > *'* t
-x>- .,. ป.'
'"/-, -7'
V .;'';;;
j* * .*'.'
.- ' .
-/> fr'f^
^^s/5
7/-^
,
Gas Meter
Reading
" ""^ '* * l'f\
"'.' ' ; . -:'-,
' \ >..*.
V//ป 6
*"" ^ /"-''^ ป"*^ *** "V
^iaxja
f j V.-B' & P &'*,$
^Sf**V*"j y /i-/
^' j *i i? t ^ ' d,i^.
.^W*a
ftQ^'l
V//tD
J/24'
?/V/5
PY / 0 ' >'
ซ>
*" " if- "" * 9* ฃ 'j - ' ""-*
.
^mCL-^iZ
Stack
Velocity
Head
C"H20)
(- , '-'.
/' i
1 '-i
ฃ1^/7
r/"^. *" '-j '*
C^ * . ' ~\
r> ป,';>o
****
ซ5ป 7o
iO "7 ^
t..y ? ? .,*
a . 76
o < f\&
--"'\ *:""'S
Ct l/O
D. ฅo
o. *^.s
o. 2>a
^'e ^J
ฃ>T3
.Meter
Orifice
Press .Biff,
C"H20)
Gale. 1 Actual
. '
'' '''"A
ti '
C ! . / c',
o.Vh"
(. ^ 1 ' '
f"\ = ';
O<- f-f Jf-
cv7' r,n
P *.:--.)
/ ^7<-
/ y4')"
1 ป' V -'^
/t 3..fr>
/ 6->'?
/':O
$ -~-ป
Stack Gas
Temp.
//: f;
/ f
/ru
y^ฃ
/rt ฃ
'/do
/d"/
/c7-
A* 7
* A *""^
1 " -i
//-i /
AT 7
7n"'/
/ C*~ *'
A- -'A
/ซ: '.v
' J-Of?
/&-$
Gas Sample
Temp. @ Dry
Gas Meter
In
, /
}
;;"i
-o- 1
y/
", '/
oV
^>
r:?
f/3
^vi
-i .."i
<" -5
'''' "^
'"""
? ^
f .' -ซ'
ฃ'3
S$
Out
': i"f
y<")
>/ *:
^G
t%1 '"'
va
'.; ,-,
e)Ac:i
J? /
*;- *
*; ,C
:'"' /
(/-, 1
i' - /
r I
.#/
1^
Sampte
<^ox,.
.-^^
]
/.--^
;rj.,c
A'/c'J
'i j * \
cf/>
^"7 ^
4 - ; ,*'
f * ' '"'
/ / ,'4>
'&' * '.' -
$'^>
7" * V
/;, . 6
/'/''.
/..o
?&
'&&
Last
Impinger
Temp c
-77
"*" -
, -,
.. ... .
,,.. ,
f- 5
^
v-~-
,.,.
r/o
-..
v. ..
" '
.V-
-
Vacuum
on
Sample
Train
;' ,';
:'.-'
/ / ,'
/' '.,'
/ ' 1
, ' |
ljt /.
:' -'
*?-' ",
' ,
l.t t :
'"' -,
~r . r
f * >
* .'
ป ; f
! * ,
<^S
-------
Gainesville, Florida
SOURCE SAMPLING FIELD DATA SHEET
Plant
Sampling Location ?' ' !.. .- :
Date .-.-" ' Run No. -''
(o\
Time Start ' ' Time End *','"'>
f ' t !
Sampling Time/Point - ป' "" / " ~* ( f
DB ฐF, WB ฐF, VF @ DP **~
Moisture 33%, FDA ' .' , Gas Density Fact or "
Barometric Press Zr-^'Hg, Stack Press Z.&&
Weather v ' ' .'' " - ''
* S\ '
(- '.-/
"Hg
"Hg
Temp, ; ' ฐF, W/D ,W/S
ป
Sairole Box No. ' Meter Box No.
Meter AHS ' Pitot Corr. Factor '-;/.'-'
Nozzle Dia. 7 in., Probe Length , ;
* ^
ft
Probe Heater Setting
Stack Dimensions: Inside Diameter ^7-3
Inside Area -*.,, >\ ,-
Height . '.
in
r't^
tt
f/f*f^*s
t;
, ,
t /' A f> . ^ , /
Mat'l Processing Rate
Final Gas Meter Reading
Initial Gas Meter Reading
Total Condensate in Impingers
Moisture in Silica Gel
ml
Silica Gel Container No.
Orsat: C02
02
CO
N2
Filter No.r
Excess
Air
Test Conducted by:
Remarks:
Port and
Traverse
Point No.
&&*\
^^ /
1
3
0
S"
t
s
Distance .
from End
of Port
(in.)
/-. '
/ "Y
/ ' ';
* ป ' ' ' t
i ' ' f
i
Clock
Time
0%'*tS
,* , * >
, * .
Gas Meter
Reading
(ft3)
t&'^g
-^
' * '
" ' i
; .
. '
i ...'
Stack
Velocity
Head
C"H20)
o;ss>
&* -;--:>
- .
t y
i
<
1
- -~-
Meter
Orifice
Press. Diff.
("IbO)
Calc.
/ -',
'^
, 'Fy
i
1 ,
Actual
^A/
;/,/
v ป
. . "i
/.- ^
. '
Stack Gas
Temp.
(ฐF)
//s^?
f Is /
/* /: "Lvd'
#44 f
!
' *
' ", ' '-
/rM
i ,
ซ _J
Gas Sample
Temp.@ Dry
Gas Meter
(ฐF)
In
**.-j
i
T '
;
7/
...
Out
/- X
* *
/" ,/
,- ' -1
.<"/'
^*
. ' t
Sample
Box
Tempv.
CฐF)'
(!
ฃ.5
^' c>
1 '
A- '
/ ' . '
>
Last
Impirger
Test
(ฐF)
>...._
' /
^t^
Vacuum
on
Sample
Train
("Hg)
'4.<
.'-.. ..i^1"
** ' i-*
?
-------
Port and
Traverse
Point No,
- , , -i f "
Distance
from End
of Port
(in)
t -~.
r; j (.' 77,
/ ;'
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JU
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7
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Gas Meter
Reading
(ft3)
'. t j ' i
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'7. "7"?
$'t'/t/
S77^b
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Velocity
Mead
C"H20)
Cy, l/^
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Temp.
l!C>
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167
J . ', !* j
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'71
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77
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7 -.;
7y
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-
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Temp,
A
'
/ f "' . .'*
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f
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a i
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j *
f ' I J !
'i '
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t i
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/4&
^i * . ' ' !
Last
Impinger
Temp ,
t
~
<
..-* j
v -
ป_..
77:;:
-
ป
Vacuum
#>
on
Sample
Train
f
(\
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'i
f
t
.1
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|
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-
5
y
V '.*.
1
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-------
jPort and
Traverse
jPcint No.
,(/-r^' "2..
Distance
from End
of Port
(in)
.
!&-.: ?-*1' ฃ
f
5'
i
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1 * )
Clock
Time
Gas Meter
.. Reading
.
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Stack
Velocity
Head
("H20)
,
Meter
Orifice
Press, Diff,
("H20)
Calc, | Actual
c,.,>, .-.'
I.,- .- - ' '- !
r""N. ? ''':>
1 ;
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Stack Gas
Temp , .
j
Icy
Gas Sample
Temp. 0 Dry
Gas Meter
TO
In
/ i
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on
Sample
Train
ty, ',
j
i
\
/
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1
-------
Gainesville, Florida
SOURCE SAMPLING FIELD DATA SHEET
Plant C_. /
Sampling Location^
Date
Run No.
Time Start / / >' - I Time End "-ฃ' '"
Sainpling Time/Point
DB ' 'CF, WB ฐF, VF @ DP
H
Moisture^.? I , FDA ' , Gas Density Factor
Barometric Press Zr-t"Hg, Stack Press Z/g.g"Hg
Weather .- /..
, W/D
,W/S
i'emp.__
Sample Box No. /_ Meter Box No. /_
Meter AH?
"Pitot Corr, Factor r" - '
Nozzle Dia. J.in., Probe Length
Probe Heater Setting_ --
ft
Stack Dimensions: Inside Diameter __'"Jj
Inside Area 'lf ; .
ileight ^ * ^T '
.?'':'* t'l*." " ฃ
in
tt2
ft
Mat'l Processing Rate
Final Gas Meter Reading
Initial Gas Meter Reading
ฃt3
Total Condensate in Impingers
Moisture in Silica Gel
O ml
gm
Silica Gel Container No._
Orsat: C02
02
CO
' Filter No. ,
Excess
Air
Test Conducted by: /
Remarks:
Port and
Traverse
Point No.
7 -t '' 5
K" '*' i
Distance
from End
of Port
(in.)
/ *-. .
* ป -
t ** ; ', ''
/:'-
1
Clock
Time
__
-
)| .-/:-,
; ' ' !
i
i *
t 1 L
t .
'Gas Meter
Reading
(ft3)
,.-.v-n
; -? A s-
'.- -Vl^
' v - " /
1 t
i
i :
Stack
Velocity
Head
("H20)
x?,^>.<
ff) r3 5
'." 4 ' ' ' "
i ' *
.
t. * -
Meter
Orifice
Press. Diff.
("H20)
Calc.
Xo
/ '''
f ^
? '/ f
* ~
?
f ป *
i ! -!-
Actual
* *-.:
-' T;
ป!" / -'",/
7,-'-,-,
**
.' j . .
Stack Gas
Temp.
(ฐF)
// s
// *:/>
//<
'/'/ฃ
///;
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Gas Sample
Temp . @ Dry
Gas Meter
(ฐF)
In
/.,
{*' >
i t
. , i
Out
f* ". ->
..ฃ'v.
1 ' ^
/
'. ,
Sample-
. Box,
TeiriD ,
*(ฐF)
.',.,; f
/ / ' -
-------
Port and
Traverse
Point No.
Distance
from End
of Port
(in)
. , , > ^ . '
i< c'}
ฃ 'L'S '.*
1 . >:" ''"'*
' /;;
Clock
Time
// ' '
j ,...
}/ . i, ;,
Gas Meter
Reading
(ft3)
. * . "
7V- S'- '?.
L|/6..()
' ' " ' '"! 1 f*"*
// "'/ i ' ll> ^iri.?.
'
/''I V7Vv
/ . 1 >
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; : , '/ <
t'
/ - , -1
Stack Gas
Temp .
//(
/ / -^
/"' 1 /"-'. // s
Gas Samplej
Temp.QDry
Gas' Meter
(ฐF) ' !
In
.' ) '' i
. '' i
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r, V.V. 1 /,/A A^; '//.A ! v:
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Inipingerj on *|
Temp, Sample
(CF) j Train
1
y i s ป
ti -' ! '/' <"'
FI^_ j
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Xx
s
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t
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i
i
,-
i ' -;
/ Jt - " ''
-------
Port and
Traverse
Point No.
Distance
from End
of Port
(in)
/^v&Y.
*' ' 7
*
9
/a
Clock
Time
1 "> \
i - '
) :;-:>
% y
rปr j .
Gas Meter
Reading
(ft3)
-:=,
. |f/V>^
/',:'', ซ7 '/>,', '7
' // :. 3 I';"'
72 ; ! '-"-ft
/ฃf . v \
if' ." :'-
16 - '
17 ;
i: V.
1 1 III
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' ! \ ' ' : - i j :.';'
i /;.
0 . '' '"
C^ f '. > . '
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(r?./.V o*y?l^--7*-
:
Stack Gas
Temp.
(ฐF)
i
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'// f '
^ ! ' i
/ / ' -f
f J1 i J (' - j * *
. ' U , =
i V:'.-ff rv* --'f-i 1 c'*'C'?l .-../''.
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2, A
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o f- 1 - i^'7
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<;17^*D
-^_
lbn"""flM*' f 1 / .-' ?
979./X7
: . hlK ~?'i''
i"* 7S
;':> ^ <
l/(/
/ / Ll
;; -?
Vacuum j
on i
Sample
Train
'/' />
/
-Zi_/^''a ' 1 V
'/
J *3> 3ฎ ^
, /jฃo /
'.,'-" *' ' **y (<***) I
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v.-"''-j // v; /v ' <> /
V = . :':/ //,'/
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. tS-"'l j* jj ^ ' J / f
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f. 1
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'7 -2.51 1 (
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ป. - i> 1
5LSS
^ c^-^
f y/fc,
l/S
//S
V!
-------
JNC,
Gainesville, Florida
SOURCE SAMPLING FIELD DATA SHEET
Plant
Sampling Location_
Date
/
(It::
Pain No.
Time Start
Time End
Sampling Time/Point
DB '
F, KB "/ ฐF, VF @ DP
. "Hg
Moisture g.ฃ%,FDA??._/ in., Probe Length
Probe Heater Setting -
Stack Dimensions: Inside Diameter
Inside Area ~
Height
ft
in
Tt2
" ft
+J
r* i
Mat'l Processing Rate
Final Gas Meter Reading
Initial Gas Meter Reading '-
-r
ft-5
ft3
Total Condensate in Impingers
Moisture in Silica Gel
gm
Silica Gel Container No.
Orsat: C02
02
CO
Filter No..?
Excess
Air
Test Conducted by:
Remarks:
Port and
Traverse
Point No.
?*tfl
M?l
i.
3j
Distance
from End
of Port
(in.)
( ;
1 ' '
r
Clock
Time
b$ฐ
kss
^~\
l\oS
i:(*
7 75
I;*G
Gas Meter
Reading
(ft3)
33o, ^X^*
' 33^4
"3^4.1^
- -
3ฃr3
^U^'
7:^1 ^(?7. 7
Stack
Velocity
Head
("H20)
r} . / ;
r?, ; f
/.-)
o , c^
"N C> t'
f ) ' ! S
' "- >
-
Meter
Orifice
Press. Diff.
("H20)
Calc.
. * v
V ,
-, ' '
?..'*
^ , f 0
! '
>' '
Actual
\
- - ,<",
i ป V.f
,
. 1
7./'r
\
' .
Stack Gas
Temp.
(ฐF)
74
W
*$
O' "~^
/ .,;. ..
mi
* i
9
* i <{
Gas Samt^le
Temp.@ Dry
Gas Meter
(ฐF)
In
/ /
"1 i
_ |
-/!
; i
i
-
Out
v;
v/
v/
V!
//
'/ )
,
Saraple,
Box..
Temp .
(ฐF)
~_
~-~.
. ~
_ปป
-
-
Last
Iir.pirger
Test
CฐF)
L ll(:
*ปซ-*_ป
'/7
i .
^
_-
Vacuum
on
Sample
Train
("Kg)
9.<
** * >
A'-,,r.
..
/ . .
; '
t .
'/ "
-------
Port and
Traverse
Point No,
/W^
Distance
from End
of Port
(in)
51 ;i:i --'A'
\ \
b ~7'l / '7-
,/?, . J- 4f '^ i ._______ _,
j {: f V ซ-""j " -~ "
1
a.
3
M
5
6
~" .'
"'" -* ^ *',ป
/v: ; .
>. ^ ' .1 '
Clock
Time
*-*"-}. . j
- , . ^ r-
'7 ..V ;
i ;
-; '.r-j -
''!*
\t. > ''" .,
,- j '
' : '''';
- " .
, ' / ;1
- ' . - ''
.'; ; < ]
Gas Meter
Reading
(ft3)
~- ,.,. ^ K,
V/<>'-7
7/2,:i
^- ,.
'- '!. ซ"0
"'---.-..,ป-,._..
377' 7
y. '-> i *
' ' . 5
'/? V ' 7
'-'> /
* / ! *' ' ...J
.'?!ป-. r-;
"II /. -'-
7^'>-7
-/;; r , 'ซ:'L
- i' ' '"'-.
'!'"'!,(-.)
^if>- 1'
ซ'7'7Kป fl('
Stack
Velocity
Head
C"H20)
V-^1' ^ *- '
0 . 70
..-* T- -
1. I ".'
r-. , -::-,.;>
Meter
Orifice
Press .Diff,
C"H20)
Calc,
'. ' **' <. '
Taf~ * "i ''-1'
f "*> '. *f -'
*-" i
- * ,' ;
C? , 7o -.* : .^
Actual
- ', ;;. ,-
7/>''-
;^/?o
v;'- ' f'*~ 1 .''
.-.._>- ^. _., 1 ,^,,.Jป,oซ....- i. -"- -ซซ*~-
O ป ./?.'.ซ
O . .^ /':
7 . ^--'i
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( ' * :
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^'7';.
^"''T ^ '
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*.
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1 < 9 S
a*/ ^U -.';
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[>'lฃ>
.
, ,.
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,.- . - j ,,ป P
ซ' *''"
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".. '-,'. ''
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"-',-.> "';
y-'' * '
O. s7^
.' '< ;/ -'
' ' ,
'( ' '
""v ' .>,
'>,. -
"/ "' '
"7 *? '-','
Stack Gas
Temp,
*? Z/
t/* .' ,'
cn/
. Y''/
c"/ ,' /'
-...-. -
//r?0
ซ*...
--
tf. "
h?
,,.
....
^,~,.,
/ r j
,.,.-
/O 2,
Gas Sample
Temp, @ Dry
Gas Meter
fฐF1
In
'';- j
'J t '
71
71
//.
Out
*""' *
"77
7/
?/
- / I
!
'"',''
'/:::
11
,
*"'//
7/
'?:::'.
/'
/ ''
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/J
'".-'.:
/r-
Box"> |
_
*
-
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- ...,., .
1 .,_
7^| ..ซซ.
y ;_v
7'--;
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70
'/#
71
71
7 / .
;7/
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. ซ-
.
ฐ -
ซ-,
ป_
_^
.^,
ป-ซป,
*-~
Last
Imping'er
Temp . .
yc
.....
--
-
......
f ,
7 '^
..^..
7 '
:. :-
.....
... .
I/ /'
Vacuum
.on *
Sample
Train
L/. >""
-.'' , S
-: 1
//,<:'
7/ c
j / /
/ '
7-<
/*" ,--'<
i
v -
I1 -,>
' x -7 '
/ *
' " i
v> ".
-------
Gainesville, Florida
SOURCE SAMPLING FIELD DATA SHEET
lant
amp ling Location
ate
Run No.
ime Start
Time End
ampling Time/Point
_ฐF, WB ฐF5 VF @ DP
'Hg
,FDA?7.4 ,Gas Density Factor_
arometric Pressgc/?'"Hg, Stack Press Z-f. / "Hg
'eather
.eir.p.
Sample Box No. _ '
ter AH? Pitot Corr. Factor
5F, W/D
Tt7 /C
,U/S
Meter Box No.
S'ozzle Dia.
in., Probe Length
ft
Probe Heater Setting -
Stack Dimensions: Inside Diameter
Inside Area : *
He i ght
in
Tt2
" ft
Mat'l Processing Rate
Final Gas Meter Reading
Initial Gas Meter Reading '__
Total Condensate in Impingers
Moisture in Silica Gel
ml
gm
Silica Gel Container No,
Orsat: C02
02
CO
Filter No.
Excess
Air
Test Conducted by:
Remarks:
Port and
Traverse
Point No.
fatt-l
truJ- & ?
1
3-
3
' H.
Distance
from End
of Port
(in.)
Clock
Time
&1S
r^
(f.'^n
^\$D
?.^
q\fc
c/iฃ5
9;^
Gas Meter
Reading
(ft3)
^1;^^
'" ' , , !
. i
i/Y',,o
I' V - | T
I > h ">
- ..
. ..
1 ! ft
ป ' 1
Stack
Velocity
Head
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>
*
*' <
/ * . 0
JO-o
i -
Meter
Orifice
Press. Diff.
C"H20)
Calc.
> \
^
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f : *
* / 1 .'-
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, '
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Temp.
CฐF)
I'l
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;
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V7
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Gas Sample
Temp.@ Dry
Gas Meter
(ฐF)
In
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.
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Box
Temr>.
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-
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Test
(ฐF)
".
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-
, - - -
-..
- - -
Vacuum
on
Sample
Train
("Hg)
*
" f' /
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p
/
c
/ ซ
,
-------
:;crt and
'Traverse
'Point No; '
i '"" :
' pwJ?
8 f^
'. : <-}
Distance
from End
of Port
(in)
:, ., /, ,/
i
; ' "- /
i ' '
'Clock
Time
_2i^yL
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Reading
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/r**'a \ '<'r'*
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Temp.SDty j
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(ฐF)-:' 1
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Sample'
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Temp,
V c 1 ." ' """"" 1
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70
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-------
Gainesville,: Florida
SOURCE SAMPLING FIELD DATA SHEET
aamplingiLocation f >
)ate " Run No.
lant
ime Start
Time End
Sampling Time/Point
; ฐF, \VB - c
)B
F, VF @ DP
"Hg
bis ture-2.61, FDA'yZ^. Gas Density F act or -
Barometric Pressr "Vig, Stack Press ;??. I "Hg
father
Temp. _ฐ F, W/D W/S
Sample Box No. _Meter Box No. /
Meter iH9 . Pitot Corr. Factor
Nozzle Dia. in., Probe Length
Probe Heater Setting_
Stack Dimensions: Inside Diameter
Inside Area _^
Height
ft
in
Tt2
~ ft
/Zo /<'
Mat'l Processing Rate
Final Gas Meter Reading
V.-V'/* '
Initial Gas Meter Reading
Total Condensate in Impingers
Moisture in Silica Gel
ft3
"** '
ml
gm
Silica Gel Container No.
Orsat: C02
02
CO
N2.
Filter No.
Excess
Air
Test Conducted by :
Remarks :
Port and
Traverse
Point No.
P.ifl
jfM "r-
P.'f^ฎ f
r
2-
3
Distance
from End
of Port
(in.)
i !
! Hi '
Clock
TLme
ez*.$0
/3~!.sr
a wo
a-.^s"
/^'^
/z:/r
/'6^7
L/-^
Gas Meter
Reading
(ft3)
..< -/ '77 5
/-, . .<
^v;, :^
/ /? .c
-------
?ort and
Traverse'
Point No.
/*!/ '/
, '
Distance
from End
of Port
(in)
'// //;- " "" " "" "
/7WVf ' ^ , .
, ซ*"'
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Reading
(ฃt3)'
i
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Orifice
Press, Diff.
("H20)
Gale, i Actual
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Stack Gas
Temp .
(ฐF)
J
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_/af J
//,5.^ '/.-';^
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%.-** v,^
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Temp. @ Dry
Gas Meter
(ฐF)
In
1 j : :
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/ 7
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Temp .
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-------
" ^ INF
Gainesville, Florida
SOURCE SAMPLING FIELD DATA SHEET
Plant
Samp I ing Location//'1/ ^'//' {* ("? f*' . c' / J
Date -'-'' / - Run No, /
I ' '
Time Start / ,3^ -'f> Time End ' '. / '
Sampling Time/Point '2. 5 /- ^"-' ' ' //%4> J
D3__H_ฐF> m "'' ฐF> VT @ DP O.5& "Hg
Mo i s ture ''-I, FDA '", ''; , Gas Density F act or
Barometric PressT^j'Hg, Stack PressZ&/g"Hg
.veatner_
Tern).
'F, IV/D
Meter Box No.
Sample Box No.
Meter AH@ / -^v Pitot Corr. Factor
Nozzle Dia.J'.'Vin. , Probe Length
Probe Heater Settin '
ft
Stack Dimensions: Inside Diameter -4V, "70 in
__ ^^
Inside Area
Height
Mat'l Processing Rate
Final Gas Meter Reading
ft5
Initial Gas Meter Reading
Total Condensate in Impingers
Moisture in Silica Gel
1 <
//
rnl
Silica Gel Container No.
Orsat: C02
02
CO
N2
Filter No.
Excess
Air
Test Conducted by: ..7T C'^ >
Remarks:
ft
Port and
Traverse
Point No.
/
ฃ.
y
-)
Distance
from End
of Port
(in.)
Clock
Time
'jCV-O
/ ' ' V-. * {-*
D*:>
f ~*l - * s
' /" f !_ i
. . ^ ' ^
/ฃ:?. 6
/V (9 O
*'/") \~-i .'
f .
* -t - .--*
Gas Meter
Reading
(ft3)
:'ฃy~-ซ5/.'
-/'9-A' . o
799. 6"
< ^ ." ^
* * x." *
.-. ' - /
.' ' T ," '
/
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Velocity
Head
("H20)
*,?/:^,"-r
n< <^
( / t, t- *!_
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-., "6ฐ
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"*
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Orifice
Press. Diff.
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Calc.
/LP*-
r_i\^
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/. /ซ;
' /\
T ,
Actual
^, " 0
,' I '
/. /5
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Temp.
(ฐF)
,
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S ' s
.;'.' ')
v")
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v
- , , '.-s
~"
Gas Sample j Scrrfpie-
Temp.@ Dry
Gas Meter
(ฐF)
In
j
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.
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en !
Sample
Train
("Hg)
J
*-.
8
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,
-
-------
jPort and
(Traverse'
Point No,
Distance
from End
of Port
(in)
Clock
Time
Gas Meter
Reading
(ft3)
Stack
Velocity
Head
(,"H20)
Meter
Orifice
Press. Diff.
C"H20)
Caic. Actual
Stack Gas
Temp.
Gas Sample
Temp. @ Dry
Gas Meter
In
Out
t me
Last
Impinger
Temp.
CฐF)
Vacuum
on
Sairiple
Train
$
. 21 7
A
X
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-------
Port and
Traverse
Point No.
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1 7
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7' , - '/ ,-
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Gas Meter
Reading
(ft3)
C::.. /:. A
:9^7, 5'
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7oi'7,7
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Meter
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. ("H20)
Calc.
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Temp.
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9^.
Qd.
i i
94
q4
s /r
? <-7
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9v!
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1*5 2s
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Gas Sample
Temp. @ Dry
Gas Meter
(ฐF)
In
/""?
'/,K
, * """"
7^
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77
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S? ป ป
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Temp .
(ฐF)
!<> 7c.
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(',-> <'
s - .
('.-, / .
c7 z.
:< 7"
i -; '"-.
JV~>
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Vacuum __
on
Sample
Train
/: <"
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t- -^:TJ
-------
ENVJROXMbNIAL ENGINEERING, INC,
1 ..Jine... Jle, . .brie 1
SOURCE SAMPLING FIELD DATA SHEET
Plant
Sampling Location
Date Time End //ft ; '>
(JQ-TFIL -/-'- '-' J)
5
DB
F, VF @ UP
"Hg
Mo i s tare 2 I , FDA , Gas Density F act or
Barometric Press'''' '*'Hg, Stack Press 2ฃ?/"Hg
V.'e a t he r
Te;:;p. ' ฐF, W/D
Sample Box No..
,iv/s
Meter Box No,
Meter AH9dฃ4#_Pitot Corr. Factor__
Nozzle Pi a. 0*2?)in., Probe Length
Probe Heater Setting
ft
Stack Dimensions: Inside Diameter _4-J* 7-S in
Inside Area _ it2
I ie i ght ft
Mat'l Processing Rate
Final Gas Meter Reading
"?. /-
ft5
Initial Gas Meter Reading V
Total Condcnsate in Inipingers
Moisture.in Silica Gel
ml
Silica Gel Container No._
Orsat: C02
Filter No.^i
CO _
N2 ..
Excess
Air
Test Conducted by:
Remarks:
Port and
Traverse
Point No.
'', /
-/
-^ .
v^'
; f
_
--
Distance
from End
of Port
(in.)
Clock
Time
'^ -. / -''
*" '" V-.
_..
' *,.'
."> "' ."''/ '
) " '
) '. '." '
' '' :' ^
Gas Meter
Reading
(ft3)
f^r' ft /** '' (^
^ L- ,' - ' s "! }
^ ' * " ' *
' t <
' ' ." . , ->
... , _, .
t. ' > ^ > ,'
> "* ' >-
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;, ^^ . /
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Velocity
Head
C'HzO)
/")..; ;f;.
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(ฐF)
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Velocity Orifice
Head Press. Diff, j
("H20) ("H20)
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O.I.6 0,<7
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-------
j-NViROXMLNiAL IJNGiNLIikiNG, INC,
' IGa.' la! ,lFlc'.."_;k
SOURCE SAMPLING FIELD DATA SIIJ'ET
Plant
Mat'l Processing Rate
Sampling Location ;
,-,,.,
Date
Run No,
Time Start
Time End_/J/"'; 0
f- -'"
Sampling Time/Point ; i * ' ( /f'c 7 <'''" i
DB ฐF, WB ฐF, VF @ DP "Hg
Mo i s t ure "Z. __%, FDA , Gas Deasity F act or
Barometric Press''' '-"Jig, Stack Press2g.?/ "Hg
Weather
Temp. ฐF, W/D _>w/s__^
Sample Box No.. Meter Box No,
Final Gas Meter Reading /.--.
Initial Gas Meter Reading
_ft3
ft3
:- O
ml
gm
Total Condensate in Im.pingers
Moisture in Silica Gel -
Silica Gel Container No. Filter No.;;'-; /_;
Orsat: C02
02
CO
Meter AH9
Pitot Corr. Factor . <ฃ. #3
Nozzle Dia._-_/"'in., Probe Length
Probe Heater Setting
ft
Stack Dimensions: Inside Diameter^
Inside Area
i lei girt
^\ in
it2
ft
Excess
Air
Test Conducted by:
Remarks:
Port and
Traverse
Point No. '
-.IV. '
, I i
,
L<
,
; /
Distance
from Laid
of Port
(in.)
-
Clock
Time
v ^ >
It"^',:.
,,-, ._. ...
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1 '" ,'.L "7
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Gas Meter
Reading
(ft3)
-
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, ,-;
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Velocity
Head
("H20)
(^r>-';
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Orifice
Press. Diff.
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Stack .Gas
Temp .
fF)
..." "'-%
SO
% o
% ?
:^ f(.-
.
Gas Sample
Temp . '3 Dry
Gas Meter
TO
In
-*'
7L
-/$
79
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("Hg)
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- \ - *
i
e.-r
^3
-------
[port and
Traverse
Point No.
Distance
fToni: Had
of Port
(in) .
Clock
Time
Gas Meter
Reading
'
Stack
Velocity
Head
C"H20)
Meter
Ori 1: i cc
Press. Diff,
C"1120)
Actua
Stack GasT Gas Samp 1 cT
Temp.
CฐF)
Temp. 11') ry
Gas Meter
In
Out
Las t
Iinpinger
Teinp .
Vacuum
ซ
en
Sojiiple
Train
"Vtv/CA F|
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A
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'75
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0,37
0,
0,59
-------
>I'ort and
[Traverse
Point No,
!
Distance
from End
of Port
(in)
i !
1 , r
\ :< i
i . /
^ \r*>
~
Clock
Time
Gas Meter
Reading
(ft-3)
i
/ ( ' ' t J1
1 ! 35 .ฃ>' j 9 r> t> . ฐ!
Stack
Velocity
Head
C"H20)
Meter
Orifice .
Press
,Diff,
("H20)
, Calc,
D, /4 ! i)s73
O'/f? |/?,.5Y>
Actual
0^63
Cx', /'; -',^
Stack Gas
Gas Sa.nrple! S-ar
Temp. j Temp < 9 Dry j ง
(ฐF) j Gas Meter i <ฅ
fc'F) (
I v -' f V.
9, a
9 A
In
5 -'^,
'?',
^J7'^
jO - - /. ^
3,'i /
r)i'e Last
?* Impinger
snp . Tenp .
--F) j (ฐF)
/>'/"!
^u^ { -^ .' " i
* Wtf* ! '.-"*, ; -
5" 1 :< >
Vacuum
on
Sample
T-v-" - >->
1 X dJL i 1
-------
APPENDIX D
Complete Sampling Procedures
-------
COMPLETE SAMPLING PROCEDURES FOR PARTICIPATE STACK EMISSIONS
SarnplIng Procedure
Prior to performing the actual participate emission tests,
certain preliminary stack parameters had to be estimated or determined
for the source. This preliminary data included the average temperature,
velocity heads moisture content, stack diameter, and number of sampling
points.
The stack gas temperature was determined by using bimetallic
thermometers and mercury bulb thermometers.
Velocity head measurements were determined across the stack
diameter by using a calibrated S-type pi tot tube with an inclined man-
ometer. This data was used to select the sampling nozzle diameter.
The approximate moisture content of the stack gas was deter-
mined by the wet bulb and dry bulb thermometer technique.
The sampling traverse points were selected according to Method
1 of the Federal Register (Volume 365 Number 247 ? Part II, December 23,
1971).
The stack emissions were sampled by using the following sample
train: a stainless steel nozzle; a glass-lined probe; a Gel man Type A
glass fiber filter; two impingers with 100 ml of distilled water; two
dry impingers (the second impinger had a .standard tip, while the first,
third and fourth impingers had modified tips with 1/2-inch ID openings);
-------
a thermometer on the last impinger; a'flexible sample line; an air-tight
pump; a dry test meter; and finally, a calibrated orifice with an in-
clined manometer. Figure 6 shows a schematic arrangement of the sampling
train.
Silica gel was not used in the fourth impinger because it did
not arrive with the equipment, and there was none available in the area.
After discussion with the Project Officer it was decided to test without
silica gel since the moisture was near ambient. The moisture for cal-
culations was determined by the use of the wet and dry bulb method.
Because the stack temperature was less than 100ฐF and the
moisture content was low, the probe and the filter holder portions of the
sampling train were not heated.
The impinger portion of the sampling train was iced down to
collect the condensable moisture in the stack gas.
Each point sampled across the stack diameter was sampled at an
isokinetic sampling rate.
Sample Recovery . .
Samples were recovered in accordance with procedures outlined
in Method 5 of the Federal Register (36 .F.R., March 31, 1971), Determination
of Particulate Emissions from Stationary Sources.
The sampling train glassware, exclusive of the glass lined
probe and the fritted disc filter, were soaked in chromic acid cleaning
solution for two hours previous to the preparation of sample blanks. The
probes were thoroughly washed in chromic acid solution prior to testing
-------
but were not soaked due to their cumbersome length. All sampling
glassware was rinsed extensively with distilled water following the
acid wash. . . .
All samples were turned over to the Project Officer for
additional labeling and analysis.
-------
ฃ
19
1. Nozzle
2. Probe
3. Filter .
4. Heated Compartment
5. Ice Bath
6. Impinger with 100 ml distilled water
7. Impinger with 100 ml distilled water
8. Impinger - dry
9. Impinger - dry
10. Thermometer
11. Flexible sample line
12. Vacuum gauge
13. Main control valve
14. Air tight vacuum pump
15. By-pass control valve
16. Dry test meter
17. Calibrated orifice
18.: Inclined manometer
19. "S" type pi tot tube
Figure 6.
-------
APPENDIX E
Field Test Log
-------
FIELD TEST LOG
6/18/72 Left Orlando at 1530 EDST5 arrived in Sioux City at 2230
. COST.
6/19/72 Went by to pick up equipment. Nine of the twelve boxes
made it. Probes, silica gel, toolss and umbilical cord
did not make it.
We met with Tom Ward and plant officials to discuss sampling
program. Unloaded equipment and proceeded to get material
for building stack extensions and straightening vanes.
Called office and requested additional probes.
6/20/72 Finished setting up sampling equipment and building stack
extensions.
Probes arrived at 1015. We were ready to sample the Hammer
Mill Outlet after noon. We were requested to wait until
two EPA engineers arrived so that comparative tests could
be made with the EPA train and a modified hi~vol sampler.
After the EPA sampler was set up and we leak tested our
train, we began testing at 2030. No silica gel was used.
Because the flow rate from the storage bin was not detectable
with the velometer (less than 10 f.p.m.), EPA did not re-
quest any tests using a hi-vol sampler.
Test ended at 2302.
-------
6/21/72 Second test on the Hammer Mill began at 0955, and ended
at 1145. Third test began at 1210 and ended at 1350.
We had to wait on plant process before sampling.
The first run (inlet and outlet) on the Pan Cooler began
at 1850 and ended at 2110.
6/22/72 Second run on Pan Cooler began at 0845, ended at 1105.
Third run began at 1232, and ended at 1440.
We began first test on the Column Cooler (Inlet and Outlet)
at 17259 and plant shut down 1735 and was down until 1802.
We continued sampling and finished at 1951.
6/23/72 Second test on Column Cooler began at 0750 and ended at
1000. Third run began at 1100 and shut down at 1200
because of plant shutdown. We resumed sampling at 1320
and ended at 1420.
After cleanup and packing equipment, we gave the EPA
Project Officer the samples.
6/24/72 We left Sioux City at 0730, and arrived in Gainesville
at 1530.
-------
APPENDIX F
Project Participants
-------
PROJECT PARTICIPANTS
Environmental Engineering, Inc.
Name; Title
John Koogler, Ph.D., P.E. Project Director
John Dollar, EIT, M.S. Project Manager
George Allen,, Sr. Technician Environmental Specialist
Robert Durgan, Sr. Technician Environmental Specialist
Eric Johnson, Sr. Technician Environmental Specialist
Environmental Protection Agency
Name Title .
Thomas. E. Ward Project Test Officer
Ken Woodard Project Engineer
------- |