-------
TABLE 10
Si'MMARY OF RESULTS
AMMONIA
STATION "K" - DRYER TAIL GAS SCRUBBER INLET
Run No.
Date
Barometric pressure, inches Hg
Stack pressure, inches Hfj
Stack gas moisture. % \olume
Average stack gas temperature, °F.
Stack gas flow rate @. S.T.P/SCFM.
Vol. dry gas @ S.T.P. , SCF
Ammonia, mg
Ammonia, gr/SCF
Ammonia, gr/CF
Ammonia, Ibs/hour
Ammonia Ib/ton NH^ fed
Scrubber efficiency - %
1
1-19-72
30
28.2
15.6
140
40395
3.117
0.03
0.0001
0.0001
0.05
0.005
2
1-20-72
30
28.2
15.4
130
40974
3.024
**No Lab
Data
3
1-20-72
30
28.2
14.3
133
39923
3.009
1.3
0.0066
0.0048
2.28
0.196
**
Dry, 70°F., 29.92 inches Hg,
Sample Lost
13
-------
TABLE 11
SUMMARY OF RESULTS
AMMONIA
STATION "L" - DRYER TAIL GAS SCRUBBER OUTLET
Run No.
Date
Barometric pressure, inches Hg
5- tack pressure, inches Hg
Stack gas moisture, % volume
A-'erage stack gas temperature, °F.
Stack gas flow rate @ S.T.P.*SCFM.
Vol. dry gas @ S.T.P. , SCF
Ammonia, mg
Ammonia, gr/SCF
Ammonia, gr/CF
Ammonia, Ibs/hour
Ammonia Ib/ton NH3 fed
Scrubber efficiency - %
1
1-19-72
30
30
4.3
70
47507
2.928
0.2
0.001
0.001
0.43
0.04
2
1-20-72
30
30
3
70
40512
2.927
0.4
0.002
0'.002 .
0.73
0.07
9.8
3
1-20-72
30
30
2.8
70
42851
2.869
0.3
0.002
0.002
0.59
0.05
74.1
Dry, 70°F., 29.92 inches Hg.
14
-------
TABLE 12
SUMMARY OF RESULTS
AMMONIA .
STATION "M" - COOLER TAIL GAS SCRUBBER INLET
Run No.
Date
Barometric pressure, inches Hg
Stack pressure, inches Hg
Stack gas moisture, % volume
Average stack gas temperature, °F.
Stack gas flow rate @ S.T.P.*SCFM.
Vol. dry gas @ S.T.P. , SCF
Ammonia, mg
Ammonia, gr/SCF
Ammonia, gr/CF
Ammonia, Ibs/hour
Ammonia Ib/ton NH3 fed
Scrubber efficiency - %
1
1-19-72
30
28.6
10.1
113
34385
2.939
0.03
0.0002
0.0001
0.05
0.004
2
1-20-72
30
28.6
9
130
30740
2,797
0.03
0.0002
0.0001
0.04
; 0.004
3
1-20-72
30
28.6
8.9
125
28548
2.984
0.03
0.0002
0.0001
0.04
0.003 '
Dry, 70°F.S 29.92 inches Hg.
15
-------
PROCESS DESCRIPTION
The process consists of a preneutralizer for ammoniation of wet-process
phosphoric acid, an ammoniator-granulator, and accessory equipment for drying,
cooling, and screening the product. The primary reaction is as follows:
2 NH3 + H3P04-MNH4)2 HP04
Unabsorbed ammonia gas flows out with exhaust gases; however, most of this
ammonia is returned to the process by means of a scrubbing system using weak
phosphoric acid as the scrubbing medium.
The scrubber acid is mixed with 54 percent P20r acid (from the wet-acid
plant) in the preneutralizer resulting in a solution usually averaging about
39 percent P?0r.
The DAP slurry is pumped from the reactor to the granulator where additional
ammonia is added along with recycled product to form a solid material averaging
18 percent N and 46 percent PO^C- Tnen it is dried, cooled, and screened before
being conveyed to storage.
PROCESS OPERATION
Run #1 was conducted on January 19, 1972, from 1:45 to 3:45 p.m. Process
operation was normal for the duration of the run. Run #2 was conducted under
normal process conditions from 9:30 to 11:20 a.m. on January 20. At the end
of Run #2 a lump in the granulator forced a cutback to half rate which caused
the test to be terminated ten minutes early. Run #3 was started at 1:48 p.m. the
same day and completed at 3:48 p.m. under normal operating conditions.
16
-------
\
LOCATION OF SAMPLING POINTS
The sampling sites and number of traverse points were
selected as per "Method I - Sample and Velocity Traverses for Sta-
tionary Sources, Part 60, Subchapter C, Chapter 1, Title 40," Federal
Register. No. 247-Pt. II-l.
The above method suggests using two perpendicular diameters
of traverse points per sampling station, however, on-site conditions
necessitated the use of only one traverse diameter. The suggested
number of traverse points per diameter was used where possible without
sampling within one inch of the inner wall.
Figures 2 through 7 are schematic diagrams of the stack
configurations near the sampling location, and the sampling points
traversed during the emission tests.
17
-------
>8 Dia.
>10 dia.
1_
.Port
Diameter = 3 ft
Traverse Point
1
2
3
4
5
6
Distance from
Inner Wall (in.)
TI72
5 1/4
10 5/8
25 3/8
30 3/4
34 3/8
FAN
FIGURE 2
LOCATION OF PORT, STATION I, BORDEN CHEMICALS
18
-------
Diameter =2.5'
5' cz^a 10'
r
i
£ Port
Traverse Point
1
2
3
4
5
6
7
8
9
10
11
12
Distance from Inner Wall (ft)
0.14
0.25
0.37
0.50 '
0.67
0.92
1,
1.
2.
59
83
00
2.14
2.25
2.36
FIGURE 3
LOCATION OF PORT, STATION J, BORDEN CHEMICALS.
19
-------
Diameter = 5.5 ft
Port #1'
-Port #2
Traverse Point
1
2
3
4
5
6
7
8
9
10
11
Distance from
Inner Wall (ft.)
. 0.12
0.37
0.65
0.97
1.
1.
3.
38
95
55
4.13
4.53
4.85
5.13
5.38
FIGURE 4
LOCATION OF PORT, STATION K, BORDEN CHEMICALS
20
-------
Stack
Stack
Port
Distance from
Traverse Point
1
2
3
4 '
5
6
7
8
.Inner Wall
3
9
IS
21
27
' 33
39
45
(in.)
Side View
FIGURE 5
LOCATION OF PORT, STATION L, BORDEN CHEMICALS
21
-------
Diameter = 5.5 ft
Port #1'
Port #2
Traverse Point
1
2
3
4
.5
6
7
8
9
'10
11
12
Distance from
Inner Wall (ft)
0.12
0.37
0.65
0.97
1.38
1.95
3.55
4.13
4.53
4.85
5.13
5.38
FIGURE 6
LOCATION OF PORT, STATION M, BORDEN CHEMICALS
22
-------
A
Port
Traverse
Point
1
' 2
3
4
5
6
7
8
9
10
11
12
13
Distance from
Inner Wall
(inches)
6
12
18
24
30
36
42
48
54
60
66
72
78
FIGURE 7
LOCATION OF PORT, STATION U, BORDEN CHEMICALS
23
-------
r SAMPLING AND ANALYTICAL PROCEDURES
A. Preliminary Moisture Determination
The preliminary moisture content of the stack gases at each
sampling site was determined by Method 4 of the Federal Register
(Volume 36, Number 247, Part II, December 23, 1971).
The only significant difference between F.R. Method 4 and
the method used was the configuration of the sampling train (see
Figure 8 ). The sampling train used in these tests consisted of the
first two midget impingers with 5 grams of distilled-deionized water
followed by two dry midget impingers in place of a silica gel cartridge.
After completing the moisture run, the total impinger liquid
plus water rinsings of the probe tip through the fourth impinger were
placed in an 8 ounce polyethylene container. The samples were held by
EPA personnel for further analyses.
Field data sheets are contained in Appendix B.
B. Preliminary Velocity Determination
Method 2 of the above mentioned Federal Register was used as
a guide in determining the preliminary stack gas velocity for each source
tested. The major difference was that only the maximum and minimum
24
-------
velocity heads across each stack area were determined so that a proper
nozzle size could be selected. During each of the three fluoride
emission tests, velocity head readings were taken at points selected
by using Method 1 of the Federal Register.
Stack pressure and temperature measurements were also made
during the preliminary velocity determinations.
C. Sampling for Fluoride Emissions
The sampling procedure used for determining fluoride emissions
was similar to Method 5 of the Federal Register. The major difference
between the two methods was the configuration of the sampling train.
The sampling train described in the Federal Register has a heated box
containing the filter holder directly following the glass probe. The
sampling train used in these tests contained no heated box and the filter
holder was placed between the third and fourth impingers (between dry
impinger and silica gel impinger).,to prevent sample carry-over. Figure 9
is a schematic diagram of the sampling train used.
After the selection of the sampling site and the minimum number
of sampling points per Method 2 of the above mentioned Federal Register,
three separate test runs were performed. For each run, the required
stack and sampling parameters were recorded on field data sheets. They
are included in Appendix B. Readings were taken at each traverse point
at least every 15 minutes, and when significant changes in stack para-
N
meters necessitated additional adjustments to maintain an isokinetic flow
rate. Nomographs were used to aid in the rapid adjustment of the sampling
25
-------
rate. The traverse points were selected to maintain at least one inch
from the inner stack wall.
After each run, the liquid volume in the first three impingers
was measured volumetrically and the silica gel was reweighed. The im-
pinger liquid, the filter, plus the water washings of the probe and other
sampling train components up to the silica gel were placed into poly-
ethylene containers. During some runs the different sample fractions
were placed in separate containers, while during others, all of the re-
covered sample was placed into one container. Field data sheets are
included in Appendix B.
D,. Sampling and Analytical Procedure for Ammonia
Ammonia was collected from the stack gas stream by passing
the gas through three series-connected midget impingers containing 15 ml
of IN sulfuric acid. Ammonia is quantitatively recovered as ammonium
borate by using a modified Kjeldahl distillation procedure. The sampling
procedure was conducted per the EPA Officer and is very similar to the
procedure described by Decker and Hogan in the U.S.P.H.S. publication
"Determination of Ammonia in Stack Gas." . .",: .n, ,
The apparatus consisted of a heated glass probe, midget im-
pingers, pump, rotameter, and a dry gas test meter assembled as shown
in Figure 10. Glass wool was placed in the end of the probe to act as
a filter. Glass ball joint connectors were used between the probe and
impingers. The first three impingers contained the absorbing reagent
\
and the fourth impinger was left dry to collect any entrained liquid.
26
-------
The sampling train was leak tested prior to sampling by plugging
the inlet of the first impinger and then letting the pump create a
vacuum on the system and then recording any movement of the dry test
meter.
Due to the sensitivity of the analytical method only a small
sample was required. The sampling rate was maintained at approximately
0.1 CFM for a 30 minute sampling time.
After each of the three sample runs, the total impinger liquid
plus a distilled water rinsing of all four impingers was placed into an
8 ounce polyethylene jar for storage. ; c
Field data sheets are contained in Appendix B .
E. Liquid and Product Grab Samples
Periodically, during each test run, grab samples of the raw
materials, finished product, and scrubber liquid were taken, and the
temperature and pH were determined at the site. On some .occasions,
the samples were split with the plant, personnel' so that comparative
analyses could be performed. • : •; : . :
F. Laboratory Analysis Procedures
Water soluble fluorides were done by a sulfuric acid distilla-
tion followed by the SPADNS-ZIRCONIUM LAKE METHOD. Water insoluble
fluorides were first fused with NaOH followed by a sulfuric acid distilla-
tion then by the SPADNS-ZIRCONIUM LAKE METHOD.
27.
-------
Ammonia is quantitatively recovered as ammonia borate by
using a modified kjeldahl distillation procedure. The ammonia samples
were split with plant personnel. The analyses done by the Environ-
mental Protection Agency are reported.
PpOg analysis of the stack effluent was done by EPA personnel
For more details of exact method used, see Appendix C.
28
-------
1. Heated Glass Probe
2. Glass Connector
3. Ice Bath
4. Midget Impinger With
5. Midget Impinger With
6. Midget Impinger,
7. Midget Impinger,
8. Flexible Sample Line
9. Vacuum Gauge
10. Main Control Valve
11. By-Pass Control Valve
12.' Air Tight Vacuum Pump
13. Dry Test Meter
14. Thermometer
15. ' Calibrated Orifice
16. •Inclined Manometer
17. S-Type Pi tot Tube
Figure "'8
MOISTURE SAMPLING.TRAIN
-------
1. Stainless Steel Nozzle
2. Heated Glass Probe
3. Glass Connector
4. Ice Bath
5. Impinger with 100 ml HLO (Modified Tip)
6. Impinger with 100 ml HgO (Standard Tip)
7. Impinger, Dry (Modifiea Tip)
8. Impinger with 180 grams Silica Gel (Modified Tip)
9. Filter Holder with No. 1 Whatman Filter
10. Thermometer
11. Flexible Sample Line .
12.. Vacuum Gauge
13.- Main Control Valve
14. By-Pass Control Valve ' .
15. Air Tight Vacuum Pump.
16.- Dry Test Meter
17. Calibrated Orifice
18. Inclined Manometer
19. S-Type Pitot Tube
Figure 9
FLUORIDE SAMPLING1 TRAIN
-------
1.
2.
3.
4.
5.
'6.
7.
8.
9.
10.
11.
12.
13.
14.
Nozzle (Optional)
Heated Glass Probe with Glass Wool as Filter
Ice Bath
Midget Impingers Containing 15 ml INTLSCL
Midget Impingers Containing 15 ml INH-SCL
Midget Impingers Containing 15 ml INH-SO,
Dry Midget Impinger
Flexible Sample Line
Drying Tube
Pump • . .
Control Valve
'Rotameter .,-'.-• • • .
Dry Test Meter • • .
Thermometer . .
11
FIGURE 10
AMMONIA SAMPLING TRAIN
-------
APPENDIX
-------
APPENDIX A
Emission Calculations & Results
-------
E.E.I. SOURCE SAMPLING NOMENCLATURE SHEET
PB - Barometric pressure, inches Hg
PS - Stack pressure, inches Hg
As - Stack area, sq. ft.
AS'- Effective area of positive stack gas flow, sq. ft.
NPTS - Number of traverse points where the pitot velocity head was greater than zer<
TS - Stack temperature, °R
TM - Meter temperature, °R
H - Average square root of velocity head, finches ^0
. AH - Average meter orifice pressure differential, inches ^0
AN - Sampling nozzle area, square feet
CP - S-type pitot tube correction factor
VM - Recorded meter volume sample, cubic feet (meter conditions)
VC - Condensate and silica gel increase in impringers, milliliters
Po - Pressure at the dry test meter orifice, fPB +A. H~| inches Hg
L 13.6J
STP - Standard conditions, dry, 70°F, 29.92 inches Hg
Conversion of condensate in milliliters to water vapor in cubic feet (STP)
Volume sampled, cubic feet (STP)
Total water vapor volume and dry gas volume sampled, cubic feet (STP)
Moisture fraction of stack gas
Dry gas fraction
Molecular weight of stack gas, Ibs/lb-mole (dry conditions)
Molecular weight of stack gas, Ibs/lb-mole (stack conditions)
Specific gravity of stack gas, referred to air
Excess air, %
Average square root of velocity head times stack temperature
Stack gas velocity, feet per minute
Stack gas flow rate, cubic feet per minute (stack conditions)
Stack gas flow rate, cubic feet per minute (dry conditions)
Stack gas flow rate, cubic feet per minute (STP)
Percent isokinetic volume sampled (method described in F.ederal Register)
Total Sample Time (minutes)
-------
EQUATIONS FOR CALCULATING FLUORIDE EMISSIONS
VWV = (0.0474) x (VC)
VSTPD = (17.71 x (VM) x (PB + AH_ ) ^_ TM
13.6
VT = (VWV) + (VSTPD)
W = (VWV)-r(VT)
FDA = (1.0) - (W)
FMOIST = Assumed moisture fraction
MD = (0.44 x % CO ) + (0.32 x % 0£) + (0.28 x % N2) + (0.28 x % CO)
MS = (MD x FDA) + (18 x W)
GS = (MS)-r- (28.99)
' EA = [(100) x (% 02 - ^2^)] -i- Qo.266 x % NZ) - (% 02 - %2C°)]
U = (174) x (CP) x (H) x A/(TS x 29.92)-j-(GS x PS)
QS = (U) x (AS) ;
QD = (QS) x (FDA)
QSTPD = (QD) x ( 53°) x (?-§.)
29.92 TS
PISO = (o.oo267 x VC x TS) + (PQ x TS x VM-^-TM) ~ (Time x U x PS x AN)
Fluoride Emissions:
MG = Milligrams of fluoride from lab analysis
Grains/SCF = (0.01543) x (MG) -f- VSTPD
Grains/CF, Stack Cond. = (17.71) x (PS) x (FDA) x (Grains/SCF) -7- (TS)
Lbs/hour = (Grains/SCF) x (0.00857) x (QSTPD)
- P2°5 Fed = Tons/hour, determined from plant data "
Lbs/ton P2° Fed = (Ibs/hour)-J- (Tons/hour P0e Fed)
-------
EQUATIONS FOR CALCULATING AMMONIA EMISSIONS '.
VSTPD = 17.71 x VM x (PB + yj^-) * TM
FDA = obtained from fluoride emission test
QSTPD = obtained from fluoride emission test
Ammonia Emissions:
Mg = Milligrams of NH3, determined from lab analysis
Grains/SCF = (0.01543) x (MG) -j VSTPD
Grains/CF, Stack Cond. = (17.71) x (PS) x (FDA) x (Grains/SCF) * TS
Lbs/hour = (Grains/SCF) x (0.00857) x (QSTPD)
NHg Fed = Tons/hour, determined from plant data
L'bs/ton NH3 Fed = (Ibs/hour) -j (tons/hour NH3 Fed)
-------
FLUORIDE EMISSIONS
-------
no OF nuns
TEST 110 -
PLANT - BORDEN CHEMICAL PINEY POINT, FLA.
SOURCE - REACTOR SCRUBBER INLET I
TYPE OF PLANT - D.A.P.
CONTROL EQUIPMENT -
POLLUTANTS SAMPLED - FLUORIDES
- 3
1)RUN liW'BER
2 ) DA TE
3) TIME BEGAN
H)TIME END
^BAROMETRIC PRESSURE, IN UG
&)METER ORIFICE PRESSURE DROP, IH HG
1)VOL DRY CAS, METER COND, CUBIC FEET
8) AVER AGE GAS METER TEMPERATURE, DEC F
9)KOL DRY GAS, S.T.P. , CUBIC FEET
10) TOTAL 1120 COLLECTED, III
11) VOL 1120 VAPOR COLLECTED, S.T.P. , CU FL
12) STACK GAS MOISTURE, PERCENT VOLUME
12) ASSUMED STACK GAS MOISTURE, PCT VOL
Ik) PER CENT C02
l\j)PERCENT 02
17) PER CENT N2
IB) PER CENT EXCESS AIR
13)MOLECULAR HEIGHT OF STACK GAS, DRY
20)MOLECULAR WEIGHT OF STACK GAS, STK CO in
21 )S TACK GAS SPECIFIC GRAVITY
22)AVG SQUARE ROOT (VEL HEAD), IN H20
23)AVERAGE STACK GAS TEMPERATURE, DEG F
2H)AVG SQUARE ROOT- (STK TEMP*VEL HEAD)
2S)PITOT CORRECTION FACTOR
2b)STACK PRESSURE, IN HG, ABSOLUTE
21) STACK GAS VEL, STACK COND, F.P.ti.
2B)STACK AREA, SO FEET
2B)EFFECTIVE STACK AREA, SQUARE FEET
30)STACK GAS FLOW RATE, S.T.P. , SCFMD
•31)f/ET TIME OF TEST, MINUTES
32)SAi-:PLIn'G NOZZLE DIAMETER, INCHES
33)PERCENT ISOKINETIC
•3 ii \ 71 r / //*) rj 7* n *"' r/^r^7"':O r'/^rr/Dr1"1 / '/"*
34 ;/' LUUii 1 !>u - HtuLK bOLUoLL,, /•/(/
35) FLUORIDE - TOTAL, MG
3&)FLUORIDE - WATER SOLUBLE, GR/SCF
37) FLUORIDE - TOTAL, GR/SCF
3U)FLUOi:iDE - WATER SOL., GR/CF, STK CUD.
39) FLUORIDE - TOTAL, CR/CF, STK CUD..
HO)FLUORIDE - WATER SOLUBLE, LB/HOUR
HDFLUORIDE - TOTAL, LU/HOUR
HDFLUORIDE - WATER SOL., Lti/TOU F205 FED
i 1 -
J_ 13:45
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___ ..
1JL0332___ JO.,02]4 _LO_._P.D2L __
vo DEGI;EES F, 20.92 I;:CUES MERCURY***
-------
1QU&CL TEST DAU
TEST NO - • HO OF PUNS
PLANT - BOPDEN CHEMICAL PIIJEY POIUT, FLA.
SOURCE - REACTOR SCRUBBER OUTLET J
TyPE OF PLAUT - D.A.P.
COHTROL EQUIPMEHT -
POLLUTANTS SAMPLED - FLUORIDES
- 3
2
3
5
6
7
8
9
10
. 11
12
17
19
20
21
22
24
25
)RUil i'JUMBER
)DATE
) TIM IS BEGAK
^BAROMETRIC PRESSURE, It! II G
)METER ORIFICE PRESSURE DROP, IK HG
)VOL DRY CAS, METER COUD, CUBIC FEET
) AVER AGE GAS METER TEMPERATURE, DEC F
)VOL DRY GAS, S.T.P. , CUBIC FEET
) TOTAL 1120 COLLECTED, ML
)VOL 1120 VAPOR COLLECTED, S.T.P. , CU
)STACK GAS MOISTURE, PERCENT VOLUME
)ASSUMED STACK GAS MOISTURE, PCT VOL
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) STACK
)STACK
PRESSURE, li! HG, ABSOLUTE
GAS VEL,. STACK COKD, F.P.H.
AREA, SQ FEET
^EFFECTIVE STACK AREA, SQUARE FEET
) S TA CK GA S FLOW RATE, S.T.P.
)NET TIME OF TEST, MIUUTES
)SAMPLIrJG NOZZLE DIAMETER,
)PERCEHT ISOKIUETIC
3H)FLUORIDE - WATER SOLUBLE,
3S)FLUORIDE - TOTAL,
WATER SOLUBLE,
TOTAL,
UATER SOL.
TOTAL,
l-.'A TER
TOTAL
_ _1_3£
i 2^"7l^~8 1_1^.1 1_"LL __
.r.Tn^i r^rnT i~~
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CFMD
HG
MG
GR/SCF
) FLUORIDE
)FLUOI-:iDh'
) FLUORIDE
l
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— ~
I T
"
H3
«»«*
) FLUORIDE
)FLUORIDL'
) FLUORIDE
GR/SCF
GR/CF, STK
GIUCF, STK
SOLUBLE, LB/HOUR
LB/HOUR
0"rO~0~n5
i
CUD,
CUD,
- UATLIR SOL,
- TOTAL,
/TOI!
P205
P205
FED
1_QJJ5Q1 ____ I_cu2aa
1_ ___ 1 _______ . ____ 1 ___ ,
1_0.-.9.181 ____ 1_0-_QPI3 ____ i_
J._0.bl81 __ i_0.0073. ____ 1JLD114. ____
***S.T.l'. *»*DHX , 70 DEGREES F, 29.92' IVCUES
-------
IQURCE ££££ £4£4
PLANT - BORDEI! CHEMICAL
SOURCE - DRYER OUTLET L
TYPE OF PLANT - D.A.P.
COUTROL EQUIPMENT -
POLLUTANTS SAMPLED - FLUORIDES
no OF nuns
PI11EY POINT, FLA.
- 3
DRUi! UUl'BER
2 ) DA TE
3) TIME BEG A!,'
5)BAHOMETRIC PRESSURE, It! JIG
S)1>1ETEX ORIFICE PRESSURE DROP, IH F.G
7) VOL DRY CAS, METER COUD, CUBIC FEET
B) AVER AGE GAS METER TEMPERATURE, DEC F
9) VOL DRY GAS, S.T.P. , CUBIC FEET
10) TOTAL !: 20 COLLECTED, ML
1DVOL H20 VAPOR COLLECTED, S.T.P. , CU F'.
12) STACK GAS MOISTURE, PERCENT VOLUME
13) ASSUMED STACK GAS MOISTURE, PCT VOL
IH) PERCENT C02
1S)PERCEHT 02
It) PERCENT CO
17) PERCENT 112
1B)PERCE11T EXCESS AIR
19) MOLECULAR WEIGHT OF STACK GAS, DRY
20)MOLECULAR WEIGHT OF STACK GAS, STK COUl
21} STACK GAS SPECIFIC GRAVITY
22)AVG SQUARE ROOT (VEL HEAD), III 1120
23)AVERAGE STACK GAS TEMPERATURE, DEC F
2H)AVG SQUARE ROOT (STK TEMP*VEL HEAD)
2S)PITOT CORRECTION FACTOR
2b)STACK PRESSURE, HI HG, ABSOLUTE
2DSTA CK CAS VEL , STA CK COUD , F.P.M.
2B)STACK AREA, SQ FEET
23)EFFL:CTIVE STACK AREA, SQUARE FEET
30)6' TA CK GA S F LOW RA TE , S.T.P. , S CFMD
31)NET TIME OF TEST, MINUTES
32)SAiWLI!lG NOZZLE DIAMETER, INCHES
3 3 ) PERCEil T ISOKI11ETIC
34) FLUORIDE - WATER SOLUBLE, l-IG
3S)FLUORIDE - TOTAL, MG
3b)FLUORIDE - WATER SOLUBLE, GR/SCF
S'l) FLUORIDE - TOTAL, GR/SCF
3n \ r7 r Tin r.> T r> :•' 'r/i r;".~r>
-------
.QURCE TEST DATA
TEST no- • no OF nuns- 3
PLANT- FORDEM CHEMICAL PII'lEY POINT, FLA.
SOURCE- COOLER IflLET M
TYPE OF PLA11T- D.A.P.
CONTROL EQUIPMFNT-
POLLUTA11TS SAMPLED- FLUORIDES
1)RU.; NUMBER
2 ) DA TE
4 ) TIME El'iD
5)BAROMETRIC PRESSURE, II! UG
&)METER ORIFICE PRESSURE DROP, IK HG
7) VOL DRY CAS, METER C011D , CUBIC FEET
8) AVER AGE GAS METER TEMPERATURE, DEC F
9)KOL DRY GAS, S.T.P. , CUBIC FEET
1Q) TOTAL I! 20 COLLECTED, ML
11) VOL H20 VAPOR COLLECTED, S.T.P. , CU F'.
12) STACK GAS MOISTURE, PERCENT VOLUME
13) ASSUMED STACK GAS MOISTURE, PCT VOL
14 ) PERCE iJT C02
llJ>)PERCEi!T 02
1 6 )PERC EIST CO
. 11) PERCENT U2
IB) PERCENT EXCESS AIR
13)MOLECULAR WEIGHT OF STACK GAS, DRY
2Q)fJOLECULAR WEIGHT OF STACK GAS, STK COUl
2DSTACK GAS SPECIFIC GRAVITY
22)AVG SQUARE ROOT (VEL HEAD), 1/7 7/20
2 3 ) A VERA GE S TA CK GAS TEMPERA TUR E , DEC F
2H)AVG SQUARE ROOT (STX TEMP* VEL HEAD)
2S)PITOT CORRECTION FACTOR
26)STACK PRESSURE, 1/7 UG , ABSOLUTE .
27) STACK GAS VEL, STACK COIJD, F.P.M.
2B)ST^CK />REA, SQ FEET
23)EFFECTIVE STACK AREA, SQUARE FEET
30)STACK GAS FLOW RATE, S.T.P. , SCFM'D
31)UET TIME OF TEST, MIUUTES
32)SAi-:PLi;!C iJOZZLE DIAMETER, IUCHES
3 3 ) PERCENT ISOKIUETIC
3i\)FLUORIDE - WATER SOLUBLE, MG
3b) FLUORIDE - TOTAL, MG
36)FLUORIDE - WATER SOLUBLE, GR/SCF
3'DFLUORIDE - TOTAL, CR/SCF
3Q)FLUORID;-: - WATER SOL., GR/CF, STK CUD.
3V)FLUORIDE - TOTAL, GR/CF, STK CUD.
HQ)FLUOXIDS - WATER SOLUBLE, LB/HOUR
4 1 ) FL UORID E - TOT A L , LB /HO UR
43) FLUORIDE - WATER SOL., LH/TOii P2013 FED
i\H)FLUO;!IUV - TOTAL, LB/TOi! P201> FED
\
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62.279 156.7J9
147.5 1118^5
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28.85 128. 8
27 . 75 127. 82 '
0.96 10.96
0.509 10.45
113 1125
12.195 110. 879
0.83 10. 83
27.97 128.67
18G1 . 7 11638. 4
23.76 123.76
23.76 123. 76
34305 130740
120 I120
0. 25 1°. 25
105.2 J_107.1
"27^4"23 133723
OJ.OOGP, 10.009
n^noGR ID. 009
Oj_0053 10. 0071
0.0053 10. 0071
2.0039 12.3709.-
2.0039 12.3709
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***S.T.P.<--*-DRY, 70 DEGREES F, 29.92' II.'CI-KS MERCURY***
-------
. .V_. -. SOURCE TEST DATA " J_ -
TEST NO. - •••••- - NQ> OF RUN$ _ 3
PLANT - BORDEN CHEMICAL PINEY POINT, FLA.
SOURCE - OUTLET STACK U , , V.
TYPE OF PLANT - D.A.P. / / : ., '
CONTROL EQUIPMENT - ., ";v
POLLUTANTS SAMPLED - FLUORIDES ' - " -'
NOTE: BECAUSE OF PHYSICAL DIFFICULTY WITH THE SAMPLING PLATFORM, ONLY
THE CENTER PORTION OF THE STACK COULD BE SAMPLED. THE ABOVE
VELOCITY AND FLOW CALCULATIONS WERE BASED UPON A THOROUGH VELOCITY
TRAVERSE ACROSS THE STACK.
l)RUil HUMBER
2)DATE - .
3)TIME BEGAN
H)TIME EllD ••-.'-.
^BAROMETRIC PRESSURE, III EG .
6)METER ORIFICE PRESSURE DROP, IH HG
7) VOL DRY GAS, METER COUD, CUBIC FEET
8) AVER AGE GAS METER TEMPERATURE, DEC F
9) VOL DRY GAS, S.T.P. , CUBIC FEET
10)TOTAL 1120 COLLECTED, ML
11) VOL 1120 VAPOR COLLECTED, S.T.P. , CU FL
12)STACK GAS MOISTURE, PERCENT VOLUME
1$) ASSUMED STACK GAS MOISTURE, PCT VOL
lH)PEHCEtiT C02
1&)PERCE3T CO •
1DPERCEKT U2 " . : .
18)PERCEilT EXCESS AIR '• '
^MOLECULAR HEIGHT OF STACK GAS, DRY
20)MOLECULAR WEIGHT OF STACK GAS, STK COIJ1
2DSTACK GAS SPECIFIC GRAVITY .
22)AVG SQUARE ROOT (VEL HEAD), III H20
23) AVER AGE STACK GAS TEMPERATURE , DEC F
2 4 ) A VG SQ UARE ROOT ( S TK TEUP* VEL HE A D )
2S)PITOT CORRECTION FACTOR
26)STACK PRESSURE, HI HG , ABSOLUTE
2DSTACK CAS VEL, STACK COUD, F.P.M.
2Q)STACK AREA, SQ FEET
23)EFFECTIVE STACK AREA, SQUARE FEET
3Q)STACK GAS FLOW RATE, S.T.P. , SCFMD
31) NET T-IME OF TEST, MII1UTES
Z2)SAi-:?LIl!G NOZZLE DIAMETER, IUCHES
33) PER C [EH T ISOKIIJETIC^
3H)FLUORIDE - WATER SOLUBLE, MG
35)FLUORIDE - TOTAL, MG
WFLVORIDil - WATER SOLUBLE, GR/SCF
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• W)FLUORIDE - TOTAL, GR/CF, STK CUD.
HQ)FLUORIDE - WATER SOLUBLE, LB/UOUR
HDFLUORIDZ - TOTAL, LB/HOUR
W)FLUORIDE - WATER SOL.,, LB/TOii P20S FED
W)FLUORIDU - TOTAL, LB/TOI! P205 FED
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***S.T.P.+"+DRY, 70 DEGREES F, 29.92- IllCKES MERCURY***
tX ISOKINETIC DETERMINED USING VELOCITY HEAD-READINGS FROM ACTUAL FLUORIDE TEST, NOT
VELOCITY HEADS OF COMPLETE STACK TRAVERSE.
-------
PLANT -
sown -
F, OF PLAUT - D.A.
NO OF PUNS
PINEY POINT, FLA.
INLET K
(.(.ni j. nu a ! -i; ij j. t. • - • - -
POLLUTAUTS SAMPLED - FLUORIDES
l)A'i/;,' IWUBER
2 ) DA TE
3)2'JWi' BE GAM
UPTIME END
S)BARO V E TKI C PR ESSUn^. ,
jyij/i/tvxi-^-^-* . i-»~f-»r»r^7/K
&WETEK OH IF ICE W^W-
7)FOL z?/?y c/is, w^/? ^
8MVS/MCS G/1S METER Tk.-
Q)VOL DRY GAS , S.T.P. .
10)rOWL 7/20 COLLECT^
11)VOL 1110 VAPOR tO^L^L-
12)STACK GAS .MOISTURE, <
1VASSUU3D STACK CAS W-
!H)PERCEtiT C02
lS)Pfc';?C'iiV/r 02
WiPESczsT co
11) PERCENT A'2
ia)P^Ci'//£' EXCESS ^l*
19)/.;OLS(7i/M !/Z>TG//T OF
20)A/OL^^ f//VJC//2- CK GA S F LOW :h- * :'' '
j/7 7/C
>F DEOP, IK KG
'lllD, CUBIC FEET
•PEP AT U RE, DEC F
CUBIC FEET
TED, S.T.P. , CU F2
PERCENT VOLUME
ISTURE, PCT VOL
STACK GAS, DRy
STACK GAS, STK CO VI
PA V I Ti-
ll E AD), HI U20
•UPIWAMXE, DEG F
TEHPxVEL HEAD)
'TOR
'0, ABSOLUTE
; COM, F.P.tf.
I SQUARE FEET
,' S.T.P. , SCFMD
_..,-,- » t~*
O v / *^ -^ * * ^ •* *• „ . / *r * i i / ', ' /• •-,
nur^s ss,nf «Si?. «—
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-------
AMMONIA EMISSIONS
-------
AMMONIA EMISSIONS DATA
PLANT
STACK
PORDFIJ WJWICAL
F.y POTVT, FLA
REACTOR SfiRUPPIW IflLZT I
Run No.
Date
Time Started
Time Ended
Barometric Pressure, "Hg
Stack Pressure, "Hg
3
Final Meter Reading Ft
Initial Meter Reading Ft
0
Meter Volume (meter cond. Ft )
Gas Volume Sampled, *Ft3
Meter Temperature °F
Stack Temperature °F
3
Average Gas Flow Rate, *Ft /min
Ammonia, nig
Ammonia Ibs/hr
Ammonia Ib/ton NH3 fed
Ammonia gr/SCF
Ammonia gr/CF Stack Cond.
1
1/19/72
15:55
• 16: 25
30
28. 5
3.10
0.082
3. 090
3 . 0 4 3 1
01
160
10030
106.1
46.19
4.1241
0.53344
0.27719
2
1/20/72
13:05
13: 35
30
20. 5
973.98
970. 7
3.282
3.1711 '
90
165
9450
90.2
3 0 . R 5 5
3.4514
0.4730
0.22771
3
1/20/72
16:35
17:05
30
20. 5
46. 202
43. 409
2. 793
2. 7104
06
166
9338
71. 3
32. 325
2 . 7 0 R 6
0.4013
0.19353
* Dry, 7CTF, 29.92 "Hg
* nc.
-------
PLANT
AMMONIA EMISSIONS DATA
PIUFY POTFT <
STACK RFACTOP. SCRUTP.F.P. OUTLP.T J
Run No.
Date
Time Started
Time Ended
Barometric Pressure, "Hg
Stack Pressure, "Hg
3
Final Meter Reading Ft
3
Initial Meter Reading Ft
o
Meter Volume (meter cond. Ft )
Gas Volume Sampled, *Ft3
Meter Temperature °F
Stack Temperature F
3
Average Gas Flow Rate, *Ft /min
Ammonia, mg
Ammonia Ibs/hr
Ammonia Ib/ton NH3 fed
Ammonia gr/SCF
Ammonia gr/CF Stack Cond.
1
1/19/72
1 f> : 1 5
- 16:45
30
30
824.21
821.03
3.181
3.0404
96
131
10302
1.1
0.49192
0.043922
0. 0055355
0. 0043304
2
' 1/20/72
13:15
13:45
30
30
921 .11
918. 21
2. 893
• • 2.8003
89
130
10391
0.4
0.19589
. 0.01749
0.0021054
0. 0017165
3
1/20/72
1G: 45
17 : 15
30
30
12. 09
8. 81
3. 28
3 . 1 6 9 2
90
132
9338
0. 5
0. 19444
0. 01 676 2
0.0024139
0. 0018397
* Dry, 70°F, 29.92 "Hg
vnnirttninenfal
inc.
-------
AMMONIA EMISSIONS DATA
PLANT
POINT. FLA
STACK n/?7Ffl SCPUR1WR INLET ¥
Run No.
Date
Time Started
Time Ended
Barometric Pressure, "Hg
-Stack Pressure, "Hg
3
Final Meter Reading Ft
3
Initial Meter Reading Ft
Meter Volume (meter cond. Ft )
3
Gas Volume Sampled, *Ft
Meter Temperature °F
Stack Temperature °F
Average Gas Flow Rate, *Ft3/min
Ammonia, mg
Ammonia Ibs/hr
Ammonia Ib/ton NH3 fed
Ammonia gr/SCF
'Ammonia gr/CF Stack Cond.
1
1/19/72
17: 25
17:55
30
28. 2
20, 07
25.85 -
3. 22
3 . 1 1 6 9
89
140
40395
0. 03
0.051314
0. 0045016
0. 0001472G
0.00010348
2
' 1/20/72
13:10
13 :40
30
28.2
32.21
29.08
3.13
. • 3.0242
90
130
40974
3
1/20/72
1 6 : 45
17:15
30
28. 2
35. 35
32.23
3.12
3.0091
.01
133
39923
1.3
2.2763
0.1 96 24
0. 006 G 099
0. 0047 71 H
Dry, 70UF, 29.92 "Hg
cnvinftainvntat
, IKK-.
-------
AMMONIA EMISSIONS DATA
PLANT BORDEIJ CHEMICAL PIUF,? POINT. FLA
STACK np.ypjp scnviwr.n OUTLET L
Run No.
Date
Time Started
Time Ended
Barometric Pressure, "Hg
-Stack Pressure, "Hg
3
Final Meter Reading Ft
3
Initial Meter Reading Ft
3
Meter Volume (meter cond. Ft )
Gas Volume Sampled, *Ft3
Meter Temperature °F
Stack Temperature °F
3
Average Gas Flow Rate, *Ft /min
Ammonia, mg
Ammonia Ibs/hr
Ammonia Ib/ton NH3 fed
Ammonia gr/SCF
Ammonia gr/CF Stack Cond.
l
1/19/72
16:40
17:10
30
30
392.8
389. 71--
3. 086
2.9285
100
70
47507
0.2
0.42821
0.038233
0.0010449
0.0010027
2
1/20/72
13: 20
13:50
30
30
480. 38
477.29
3.085
1 ' 2.9275
100
70
40512
0.4
0. 73055
O.OG5228
0. 0020905
0. 0020332
3
1/20/72
IB: 25
16:55
30
30
579. 2B
576.25
3.023
j
2.8587
100
70
42851 •
1
0. 3
0. 59143
0.050986
0.0016
0. 00155H4
* Dry, 70°F, 29.92 "Hg
-------
AMMONIA EMISSIONS DATA
PLANT
?.77.7Py POTFT
STACK COOLFP. SCRUpnr.
Run No.
Date
Time Started
Time Ended
Barometric Pressure, "Hg
Stack Pressure, "Hg
Final Meter Reading Ft
3
Initial Meter Reading Ft
0
Meter Volume (meter cond. Ft )
3
Gas Volume Sampled, *Ft
Meter Temperature F
Stack Temperature °F
3
Average Gas Flow Rate, *Ft /min
Ammonia, mg
Ammonia Ibs/hr
Ammonia Ib/ton NH3 fed
Ammonia gr/SCF
Ammonia gr/CF Stack Cond.
1
1/19/72
16:00
16:30
30
28. 6
9.251
6. 20H
3. 042
2.9392
90
113
3'!-385
0. 03
0 . 0 4 P 3 2
0. 0041357
0 . 0 0 0 1 5 G 1 R
0. 00012413
2
1/20/72
13:00
13 : 30
30
28. 6
12.5
9. 6
2.9
2. 7969
91
130
30740
0.03
0. 043516
0. 0030854
0. 00016411
0. 00012023
3
1/20/72
16:30
17: 00
30
20.6
15 . 006
12.710
3. ORO
2. 9037
90
125
20540
0. 03
0. 037004
0. 0032659
0.00015304
0.00012137 .
* Dry, 7CTF, 29.92 "Hg
ettrinmmt'ntal CKffint'vrinjj, int:
-------
AMMONIA EMISSIONS DATA
PLANT
cnr.ui HAL
PIllP.Y POTIIT, FLA
STACK COIflfOf} OUTLET H
Run No.
Date
Time Started
Time Ended
Barometric Pressure, "Hg
Stack Pressure, "Hg
Final Meter Reading Ft
3
Initial Meter Reading Ft
3
Meter Volume (meter cond. Ft )
Gas Volume Sampled, *Ft3
Meter Temperature °F
Stack Temperature °F
3
Average Gas Flow Rate, *Ft /min
Ammonia, mg
Ammonia Ibs/hr
Ammonia Ib/ton NH3 fed
Ammonia gr/SCF
Ammonia gr/CF Stack Cond.
l
1/19/72
16: 08
1C : 38
30
30
600. 63
597.93
2.7
2. 6769
7 G
95
1.0G92Q
0. 03
0.15814
0. 01412
0. 00017147
0. 00015663
2
' 1/20/72
13 : 00
13 : 30
30
30
724.4
721.41
2.986
- 2.955
'77
100
99051
0. 03
0.13272
0.01185
0. 00015533
0.00013944
3
1/20/72
16: 40
17:10
30
30
853.92
8 5 0 . 7 H
3.150
3.107H
80
100
98964
0. 03
0. 12608
0 . 0 1 0 R fi 9
0. 00014769
0. 00013231
* Dry, 70UF, 29.92 "Hg
I'nfftnecring, inc.
-------
SCRUBBER EFFICIENCY
-------
BORDEN CHEMICAL
pIAMMONI.au PHOSPHATE
. Run 1
Flow:
Total fluoride:
Ammonia:
10038 (DSCFM)
0.70 (#/HR)
46.2 (#/HR)
-©-
Reactor
Scrubber
Efficiency: (F~) 45.7
(NH3) 98.9
40395
0.45
0.05
34385
2.00
0.05
Cooler Scrubber
N^
P»
Dryer
Eff:
Scrubber
10302
0.38
0.49
v,
~7
47507
3.38
0.43
-o
(49108)
106917
1.10
0.16
To atmophere
overall
efficiency:
Stack
65.0%
99.6%
-------
BORDEN CHEMICAL
DIAMMONIUM PHOSPHATE
Run 2
Flow:
Fluoride:
Ammonia:
9458 (OSCFM)
0.47 (#/HR)
38.6 (#/HR)
Reactor Scrubber
Efficiency: (F~) 66.0
(NH ) 99.5
O
40974
0.81
Dryer Scrubber
Eff:
10391
0.16
0.19
©
30740
2.37
0.04
Cooler Scrubber
40512
1.53
0.73
(48148)
99051
0.59
0.13
To atmoshpere
Stack
Overall
Efficiency:
83.8%
99.7%
-------
BORDEN CHEMICAL
DIAMMONIUM PHOSPHATE
Run 3
Flow: 9338 (j)SCFfK> f~i\
Fluoride: 0.65 <^/««O \_y
Ammonia: 32.3 (& \*£)
39923 /7\
U.44 vlx ^
2.28
28548 X-N
T "37 rM \ ^
0.04 ^-^
Reactor Scrubber
Efficiency: (F") 56.9
(NHg) 99.4
Dryer Scrubber
Efficiency: -
74.1
Cooler Scrubber
C
V
^) 42851
/ 0.51
0.59
) 9338
-^ 0.28
0.19 .
*s^
X^
s~
r^ . ^
^^ x
(46775)
©98964
0.51
A 0.13
To atmosphere
Stack
Overal 1
Efficiency:
79.3%
99.6%
-------
APPENDIX B
Field Data
-------
PRELIMINARY MOISTURE DETERMINATION
-------
PRELIMINARY CHECK FOR STACK GAS
MOISTURE CONTENT AND SPECIFIC GRAVITY
tt *f* n
Plant /^/)? ® s ^» 7 ml
Vapor Pressure Of H20 @ DP 5> /^ "Hg Stack Pressure ZB. ^ "Hg
Moisture Fraction, H?0 ^° // Fraction Of Dry Air, FDA
•Specific Gravity
•Dry Molecular Vfeight, Md = J0.>44(&;02^)] -t-^.32(^02i^ +J0.28(^N2 + CO)] =
Molecular Weight & Stack Conditions, Ms =[(Md)x(FDA)] + [?18)x(H2olj =
Specific Gravity (Referred to air), Gs = (Ms) ~- (28.99) =
-------
PRELIMINARY CHECK FOR STACK GAS
MOISTURE CONTENT AND SPECIFIC GRAVITY
__ , (p
Plant *'•*>"
&,&
Stack
Sample T!lme
Barometric Pressure
ft rt
Moisture Content — Method 1
Final Dry Test Meter Reading
Initial Dry Test Meter Reading
Dry Test Meter Volume Sampled
Average Keter Temperature
Average Meter Vacuum
3*
Average Meter.Orifice A H
Sampling Rate
Barometric Pressure ® Meter Orifice
Dry Gas Volume Sampled & ?0 °F, 29.92 "Hg_
Condensate Volume
B 9
Water Vapor Volume 3 ?0 °F, 29,92 "Hg_
Moisture Fraction, HoO 0*0*%*.
O» & 5 7
Moisture Content — Method 2
Dry Bulb Temp, //ffi °F Wet Bulb Temp.
}J Dew Point Temp._
Vapor Pressure Of H20 @ DP
Moisture Fraction, HoO @.
"Ho- Stack Pressure
Fraction Of Dry Air, FDA 0*}
Ft
."Hg
"HoO
_L?M
"He
ml
Fraction Of Dry Air. FDA
'Hg
.Specific Gravity
-Dry Molecular Weight, Md = J0o44($c02^j] +(oc32(^02][ +^.28(^N2 + CO)] =
Molecular Weight 3 Stack Conditions, Ms =j^Md)x(FDA)] + [?18)x(H20^=
Specific Gravity (Referred to air), Gs = (Ms) -7- (28.99) =
"Kg
-------
PRELIMINARY CHECK FOR STACK GAS
MOISTURE CONTENT AND SPECIFIC GRAVITY
stack
Date
Sample Time
Barometric Pressure
Moisture Content — Method 1
Moisture Content — Method 2
Dry Bxab Temp./V^ °F Wet Bulb Temp. /IS> °F Dew Point
Vapor Pressure Of H20 3 DP ^o||S "Hg Stack Pressure 3,
Moisture Fraction, HoO ,$»09f Fraction Of Dry Air, FDA
Final Dry Test Meter Reading ^,^B fa '/<£?
Initial Dry Test Meter Reading • f^^,0 &9fl
Dry Test Meter Volume Sampled ^p > _ _Ft
Dry Test Meter Volume Sampled _ $,o@H!$ Ft 3
7~~~"" /'^
_ jg _ °p
Average Meter Vacuum _ c"°a> _ "Hg
Sampling Rate _ \ _ ^ _ . LPM
Barometric Pressure © Meter Orifice _ 3&% _ "Hg
Dry Gas Volume Sampled @ ?0 °F, 29.92 "Kg _ 2.«£>/£ _ Ft3
Condensate Volume _ &Q® ml
Water Vapor Volume % ?0 °F, 29,92 "Hg _ ' —
-• Moisture Fraction, H^O °°" _ " Fraction 'Of Dry Air, FDA '===*
Vapor Pressure Of K20 <3 DP "Hg Stack Pressure ^ "Hg
Moisture Fraction, HoO /^> ^-^ Fraction Of Dry Air, FDA A
'Specific Gravity
Dry Molecular Weight, Md = ^e44(^C02^] -J-^OZC^)! + ^.28(^N2 + Coi| =
Molecular Weight @ Stack Corxiitions, Ms = [(Md)x(FDA)] -I- [CLS)x(H2oJ =
Specific Gravity (Referred to air), Gs = (Ms) -J- (28.99) = _
-------
FLUORIDE EMISSIONS
-------
Plant B$rde.n C/i*.>
DB °F, WB' • °F, VF @ DP "Hg
J.foisture/0,5 %,FDA?^.r, Gas Density Factor
Barometric Press3<3 "Hg, Stack Press' "Hg
Weather C!C'.-;K
Temp. °F, W/D , W/S
Sample Box No. Meter Box No,
Meter AH@ i.'// Pitot Corr. Factor 0. 8 5
Nozzle Dia, .&. in, , Probe Length £> ft
Probe Heater Setting :
Stack Dimensions: .Inside Diameter^-ft^, in
Inside Area ft 2
Height ft
Sketch of Stack
V
Final Gas Meter Reading 7?S*Z0S~ ftj._
Initial Gas Meter Reading y /'O.SO^2'5''^3^
Total Condensate in Impingers ^i3 f ml
Moisture in Silica Gel//.<;c f.')c-/t'1t'^--n<"' t -',.', giir\
Silica Gel Container NoJ'&f Filter No.7/o>?.?/
Orsat: C00 • // •) -•• f"
72^.^
7 3^, -7
•7 3^ « ^
x'iT • -3
Stack
Velocity
Head
("H20)
0,30
°^\
0:52-
d°4o
&7
& *3~?
Meter
Orifi
Press
~Calc.2
,
ce
.Diff.
0)
Actual
#•??
1 tfaQ
J ,^0
/>7$
/,35T
// 3&
j'2£~
/ f 23
Stack Gas
Temp.
743
lL b
Ik (a
1 & iff
1 KI fej
/£ ^
/^^
\bk
Gas Sample
Temp.g Dry
Gas Meter
In
75
£?5'
-tyo
?S
'^
7&
?b
77
»-? q
' fi
#0
&%.
Sample
Temp.
Last
Impingar
Temp.
7&
?£
tf /")
/'6f~)
] f£)
/ 1^
(fO
. *7 7
Vacuum
on
Sample
Train
("Hg)
4, $
4. £
•^,a
.r, ^
j"3 ,.^>
V»cO
7>o :
JT--21-
^'v^
-------
Port and
Traverse
Point No.
C*"
it
n
!,
4-r
>(
it
n
' 5
n
>t
a
6 ..
f f
tr
•
Distance
from End
of Port
(in)
JO-5/?*
f - \^ 'f^y
3o%
3_4%
x
Clock
Time
Gas Meter
Reading
(ft3) .
7 »S
757, a
'///!/} f 0
7(^4 ,O
7 7 / _3
77 r. ^ .
'•;'/f,.O
»_—
w_
^MS»«a»-.
7?S>2<3S~
Stack
Velocity
Head
("H20). .
• ^ •• ^ - •
/ 4 ^ :
,A ^
^4"^
• . 4-2-
•4i
e ^j £}
,60
,50
• 51
, -5=7
.SI
.51
^^^, — ~
„ -
• .6 2
•
Meter-
Orifice
Press. Diff.
("H,0)
Cal.
« — :
• —
Actual
/. V
/•- v
{.4-
/ . 4-
Jj> /"
\s$ir
l*4pS
/«k>5
1 . BS
L t3S"
/,gs
A^S"
%-,!&
•——
-**~~
/ &
:./(>£>
'/ ^
/^^
170
1-70
17®
/ 7fi
/ 7 O
— ——
—
/7o
i;
Gas Sample
Temp.@ Dry
Gas Meter
In
//?')
/6 2-
//1 5
/&4
16$
7oP
/J7g
/fl#
(Q>*j
iafj
108)
lo£
—
. —
/as
L0ut
f*1 —
F"2^
^>3
^3>
-5.r"
<£# '
.'M
V
70
*/' <-:•
<;"-:• -~5
/ •-/
7 <-'?
f^
-,-.,.
^.
-7V
Sampte
Box
Temp;
C°F)
Last
Impinger
Temp,-
9^2-
9 ^
//) 4~
;/^-
//4~
// 0
J &O
/ fi / ~}
/D4-
/ 0 4-
IQC?
?rt
**»-~*-
^-~
//^
Vacuum
on
Sample
Train
("Hg)
__^
*?
l&
/o
/c
11
J t
II
/2,C
X'SV £>
} C,O
Ll-v^-"'
Z5>G-
- — — .
- —
/6
i
-------
.WjiNfAL civuUNBcKii'SU, JLINU".
Gainesville, Florida
SOURCE SAMPLING FIELD DATA SHEET
Plant
Sampling Location
Date /-2Q-72-
Time Start
-£"
Run No.
Time End
Sampling Time/Point
DB-_I1__OF' WB — °F, VF @ DP
Mo i s ture J*)J%, FDAfc3^, Gas Density F act or
Barometric Press.Ja "Hg, Stack
Weather
Temp. *'*£?
'Hg
, U'/D
,W/S
Sample Box No.
Meter Box No.
Nozzle
Probe Heater Setting
Pitot Corr. _
in. , Probe Length
6
ft
Stack Dimensions: Inside Diameter 3(o in.
Inside Area ' tt2
Hei glit ft
Mat'l Processing Rate
Final Gas Meter Reading
Initial Gas Meter Reading
Total Condensate in Impingers
Moisture in Silica Gel ^
gm
Silica Gel Container No, 5715 Filter
Orsat: C02 Q,8 /*
02 20-Z'A
co _ O '/i
N2 __
Excess
Air
797,
Test Conducted by: \~j ^'<:'f
Remarks:
Port and
Traverse
Point No.
/
~-~
Distance
from End
of Port
(in,)
/&.
i)
M
e ''/<
' / *
Clock
Time
Gas Meter
Reading
(ft3)
fj'W?"
-7) s , /
r-,3.7
9/1.5
<",' =':. .>;
//o . 3
?/f . ?
' Stack
Velocity
Head
("H20)
&«5®
A. 59
o<4®
o*3S
•:l 40
/; .40
Meter
Orifice
Press. Diff.
("H20)
Calc.
Actual
f*G$
/,£5
fr$S
"^0
0& s
tifc
Stack Gas
Temp.
(°F)
/&8
/At
• /6$
I hi
/'b'f
'/& 7
Gas Sample
Temp,@ Dry
Gas Meter
(°F)
In
ff
94
14
°l5
?£
f6
Out
7S1
7.6
76
^9
8/
€i^
Sample
Box
Temp.
(°F)
Last
inpirger
Test
(°F)
.:-4--
70
{ 'r •,«****"''
/^
70
& !"~'
Vacuum
on
Sample
Train
("Hg)
(>.£
7. 3
7.5
A^O
f**"
•* .*
/-. C
-------
Port and
Traverse
Point No.
/:
**•>
_•;
•
5
Distance
from End
of Port
(in)
S'/,
34 yb
i,
. it
'i
Clock
Time
Gas Meter
Reading
••- • •
V2/. 6
cy/^- . £~
f AC . f
'/;?./, /-3
f -52.^
f 35; /
f'7?. 7
74-3. 6
$%
0$$
^•25
0 ^ %
'/•ob
1 . o 5
l\d®
1>VQ
^jLJ.SL
/, 7^
/./IT
/./r
/.&?
/•?«^
/*£O
Stack Gas
Temp.
/67
/ 6 7
/fati
1 & fy
/ C> ^
no
no
.no
170
I7O
170
/£?
J&3
/72-
I7D
1 7O
170
Gas Sample
Temp. @ Dry
Gas Meter
In
r
i
;-' (?
7 .-3
9' -7
Out
p//_
,:'::> ^
^ ^
t$3\ P;3
/ } /
/^; z.
/<93
/o> .<"
/Q5
/(•}<>
(01
••"'• x-s
r^5
gf^-
c?y
,3 /
>-7
^^7
(Oil, to
10 5
104-
i fi ^
/ ( / f
IQb
/Ok
J f) 7
f<9
*?£>
fo
71
4 1
f/
f
1
Last
Impinger
Temp.
(CF)
,^P>
?£
^O
Y 3
r?7
&2^
f?4-
,3£
^-f'-j
C7 <^
q p
Bb
gfa
% /,
^,5
aa
c.72-
€f&>
Vacuum
on ^
Sample
Train
-
{*•%
(,.£
x, r
'/,?
/: r'
'A(?
7, 2-
7, £>
7 O
^, 5*
^ . 5*
/; ( ^
C.&
6:5~
7>O
7.O
7?n
-------
Eiivj.AONN.LUJi.ikL L\uj.'NEEixii\J, L\u,
Gainesville, Florida
SOURCE SAMPLING FIELD DATA SHEET
Plant PCTG/6^ C n<2>?] /£&/••••• ...
Sampling Location jfoacferScntb 1/iM"- £i«L%
Date I..?,;)- 7 .?„ Run No, 3
Time Start j ', 4-$. Time End
Sampling Time/Point & j/l-i • ^ SLOcWn r j2#r,<.<'n
DB °F, WB °F, VF @ DP "Hg
Moisture $ 0 ?6 , FDA (ju , Gas Density Factor
Barometric Press 3$ "Hg, Stack Press3$5"Hg
leather C Ic0,^.-/-
Temp, .1>;;'7U,°F, W/D ,W/S
San.pl e Bex No, Meter Box No.
Vliif-o-r /i Ufa f >-•"'/ Pi +-ot- CVvrv Por--f- / ^ mlt^-
Moisture in Silica Gel *>?6* Z. /J", / r 3L$ej Sm
Silica Gel Container No, ^2 Q Filter No. 7^<93.
Orsat: C0?
02
CO
N7 y-
Excess
Air
Test Conducted by: 8Ur I/ .
All,,,,
/A 1 i iv? J.-1.
Al'^i-, T-
1 -
Remarks :
Port and
Traverse
Point No.
!
•!
'V
1 1
Distance
from End
of Port
(in.)
i '/2
0
'1
M
5/4.
Clock
Time
•J
^
Gas Meter
Reading
(ft3)
f /'<, 5" S
/ f ~> * *? **-* ^
f 7#. &
__—
W4< 7
far, 3
j^4/,j/
^' f -" ^
• Stack
. Velocity
Head
("H20)
d, fa 5
tf*tpO
o,4£
/j t ^ g°
/"•'»3sT
^.3^-
Meter
Orifice
Press. Diff.
C'H20)
Calc.
i
i
i
i
i
Actual
/, 35
/ .2-f
'')< 8&
6><&&
o, ijS^
0< 68>
Stack Gas
Temp.
i(*4-
/6&
!
i
r* 3
^&>%
"/.£>
/73
Gas Sample
Temp. 8 Dry
Gas Meter
In
fZ
ff
/•'$
/O^
//}^-
Out
?&
e-!O
4 /
i /
') L~
r?3
Sample
Box
Temp.
)
I
Last
Impinge r
Test
-gfr
?
-------
Port and
Traverse
Point No.
£-
\
<*
3
V
4-
\
/
I
!T
1
)
4/
6
Distance
from End
of Port
(in)
5/4-
11
/D^
'/
M
M
',' £. '"•• '•-
^-D /->
'(
u
I!
3D&
t/
M
t\
34 YQ
o
(\
••(
Clock
Time
•A
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Gainesville, Florida
SOURCE SAMPLING FIELD DATA SHEET
CTSampling Location
Date y —/--9. > 2_ Run No, £_
Time Start 1 /.jr. -/,/.;, Time End_
Sampling Time/Point
"Hg
DB_L»_7/'F' '|VIH X°)SF» VF @ DP
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Total Condensate in Impingers Z^-O _ ml
Moisture in Silica Gel 24&£— 2./ 7.7 -22, & j
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Gainesville, Florida
SOURCE SAMPLING FIELD DATA SHEET
i~ — ~2 I /*"*" \ / f '
Plant y)f~>j- rr-P"? LJ-Af/n. ( 'n Mat'l Processing Rate
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Gainesville, Florida
SOURCE SAMPLING FIELD DATA SHEET
Plant
Temp
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1 Start "1 M^W.Time End --I /^/y/^<
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Total Condensate in Impingers 2. 0c) ml^C
Moisture in Silica Gel ">
Silica Gel Container No.
Orsat: C07
02
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Gainesville, Florida
SOURCE SAMPLING FIELD DATA SHEET
Plant ; /!'. "%'•'- /
Sampling Locationpry^^SQtiJ'bt.r Q&f'/zf' /C
Date ; /.'~ / ? .">
Run No.
Time Start
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DB_l_^_i_OF> WB/^2. °F, VF @ DP
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Sample Box No. d..> Meter Box No.
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ft
Stack Dimensions: Inside Diameter
Inside Area ~
Height
in
Tt2
" ft
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Mat'l Processing Rate
Final Gas Meter Reading /
Initial Gas Meter Reading &O/- 2-S~.Z
Total Condensate in Impingers
Moisture in Silica
ft3
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/
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f^1
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7
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^,, IRON—* ,ITAL ^,JINK^X Ac , JUN J.
Gainesville, Florida
SOURCE SAMPLING FIELD DATA SHEET
TeniD.
Meter
lt /Lm .(/f +* ( *,s1 e-Tf-'---"—'^ sr P . Mat'l Processing Rate
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; /_ '),/?- V.^-Run No. 2~~-
: Start .{?/.•? ^V'/Time End III 5 $
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jr AH9 Pitot Corr. Factor ;%.£'.'*?
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;k Dimensions: Inside Diameter ^^ in
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Height ft
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Q fjt f, *'->•' e- • '•— '
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Final Gas Meter Reading 7/?^ .0 V"
Initial Gas Meter Reading £ 7V, ^"7
Total Condensate in Impingers cZ-.?^1
Moisture in Silica Gel S, '7
I
Silica Gel Container No, 3/3 Filter No
Orsat: C09
02
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Gainesville, Florida
SOURCE SAMPLING FIELD DATA SHEET
Plant
Sampling Location_
Date /„ ,-). ,? - 7 2~
Run No.
Time Start % ( & ft fffiime End //f, 2,
Sampling Time/Point 4T /-/-,,', ,,
DB /? 2 °F, WB/?0°F, VF @ DP
Moisture/J?T)FDA ,Gas Density Factor
—_.—^"
'Hg
Barometric Press^^L'Hg, Stack Press^,y "Hg
We a the r
Tenp, °F, W/D ,W/S
Sample Box No. Meter Box No.
Meter AH@ Pitot Corr. Factor
Nozzle Dia, ysJ in. , Probe Length
Probe Heater Setting
ft
Stack Dimensions: Inside Diameter_
Inside Area
Height
in
Tt2
" ft
',_>
9 ft3
sT" ft3
Mat'l Processing Rate
Final Gas Meter Reading §
Initial Gas Meter Reading '
Total Condensate in Impingers
/"*
Moisture in Silica Gel 23 Z. ^ —2. >&• -V- /v^nt--
Silica Gel Container No. f <£'*•/ Filter No. X^/oj-.
Orsat: C02
02
CO
N2
Excess
Air
Test Conducted by: .f
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140, 1
7^?7. t
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Ac?
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Temp.
(°F)
/iJ
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(°F)
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7 ^
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79
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Gainesville, Florida
SOURCE SAMPLING FIELD DATA SHEET
Plant
Sampling Location
Time Start
No -
Time End / 1> 0 Z.
Snmp 1 i ng T 1 me/ Po int ^
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Barometric Press JgJ'Ug, Stack Press J0_J'llg
Sample Box No,^
Meter &HQ A&0_,PitQt Corr, Factor^
Nozzle Dia.fot^in,, Probe Length^
Probe Heater •^^'^>,_^^__^_mmm
Stack Diwou
9
ft
Inside Diameter
Inside
Height
Ft2
ft
Port c-rnd
Traverse
Point No,
Distance
from End
of Port
(in.)
Clock
Time
HO
.
Gas Meter
Reading
Mat'l Processing Rate__
Final Gas Meter Reading _
Initial Gas Meter Reading gg
Total Condensate in Impingers
Moisture in Silica
ft
Silica Gel Container No.j_Filter
Orsat: C02i ____ _
°2 ™____™___
CO
Air
Test Conducted by :
T
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Remarks;
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Velocity
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Gale, Actual
Stack Gas
Temp.
Gas Sample
Temp. 8 Dry
Gas Meter
In
Out
Sample
Box
Temp .
Last
Impinge r
Test
Vacuum
on
Sample
Train
("Hg)
ho?
72-
8
Z
3
8
70
72
7 Z
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26
70
70
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70
70
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(Traverse
Point No.
Distance
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fin)
Clock
Time
Gas Meter
Reading
Stack
Velocity
Head
C"H20)
Meter
Orifice
Press, Diff.
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Calc, Actual
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Temp.
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Temp. @ Dry
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Sample
Box
Temp,
Last
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Temp.
Vacuum
on
Sample
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70
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7.5T
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Gainesville, Florida
SOURCE SAMPLING FIELD DATA SHEET
Samp 1 im> Loeati wn
Time Start
Sampling Tlma/rtf
Barometric l'rcssj;Jo"Hgf Stack Pressj.:S[£j'iig
U'cn i he r C
jn', , Probe Length^
SumpJe Box No,^^^^j'fctor Box No.^
Meter MWj^O PItot Corr. Fo
No;:"i.o Diit.6
Probe Heater Setting
Stack Dimensions: Inside Diameter^lfV^p in
Inside Area TO" """"It2
. . . ^«iiKji«»iia«a.5r?gjrfg^.K*«^fnB.M|iriiiiiii „
. Hu.ight
Mat'l Processing l^te__/_
Final Gas Meter Read.i;(g
Initial Gas Me^er Reading '??«2 .
77,
Total Condensate in Impingers
Moisture in Silica Gel ,?.,•/x.,^-
Silica Gel Container No.^S^//
Orsat: C02 _,O
02 ...3£>.0
CO __!>__
N2_
ml
r.,,
Filtcr
Excess
Air
Test Conducted
Remarks ^>^^^^^^^^^
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p^sr^*®^,,
Port and
Traverse
Point No,
Distance
from End
of Port
(in.)
Clock
Time
Gas Meter
Reading
(£t3)
• Stack
Velocity
Head
("HzO)
Meter
Orifice
Press, Diff,
C"H20)
Stack Gas
Temp .
C°F)
Gas Sample
Temp. 2 Dry
Gas Meter
Sample
Box
Temp,
Last
Impirger
Test
Vacuum
on
Sample
Train
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-------
To
Port and
Traverse
Point No.
/
,
Distance
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'(in)
•"•26
Clock
Time
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t^z$r
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Reading
(ft3)
i
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Velocity
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Orifice
Press. Diff.
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Alb
(.£6
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Temp.
(°F)
76.
Gas Sample
Temp. @ Dry
Gas Meter
ra-
in
//#
Out
fO^
Sample
Box
Temp,
ra
— •
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Temp.
(°F)
-7^
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Sample
Train
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Jtl^^^H^RJi\lVu^^^^ByLr C^^ff^MUJLJi^^^^^^ J.J i^^o
Gainesville, Florida
SOURCE SAMPLING FIELD DATA SHEET
Plant T5"STft~J~ C^
Date ( - Z-O -7"Z-—Run No, 1>
Time Start f'3^^L Time End
Sampling Time/Point $,;/-<: ^ (<> t~Ji~/0^' ' lZj©u
DB ?O °F, WB >O°F, VF @ DP "Hg
Moisture? *£"!,, FDA ,Gas Density Factor
Barometric Press ?& "Hg, Stack Press j^> "Hg
•
Weather ^\J^tco.^ "T
Temp. °F, W/D ,W/S
Sample Box No. Meter Box No.
Meter AH@ f.$) Pitot Corr. Factor &-%3
Nozzle Dia.d>02S*in, , Probe Length $* ft
Probe Heater Setting
Stack Dimensions: Inside Diameter
*VS>
Final Gas Meter Reading 5"?^. Z^"S ft3
Initial Gas Meter Reading ^BO , 37
'S~ £t3
Tota^. Condensate in Impingers V"?O mlp<
Moisture in Silica Gel •**,•/.•'. 9 ^ ^ ?.-./../"• ''"^m-
.•/_, _ ' -!_,_.-» ,-p* Vt -P^ff
Silica Gel Container No. S'O^ Filter
Or sat: C0?
No.^d>5//
720^
02
CO
N7
Excess
Air
Test Conducted by: GO ^LSO*O
T~vj CL.^SJ£ ^-»^
Remarks: l^us^ L> ^^ ^^s^rwc.^^ //O
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Traverse
Point No.
g
7
£
f
$
1
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Distance
from End
of Port.
(in.)
i
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5?J.7
5-5T/,^
^^0,5"
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Velocity
Head
("H20)
O.JO
O.SQ
041
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Orifice
Press. Diff.
("H20)
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2.70
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3.7a
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70
70
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7o
70
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Temp.@ Dry
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(°F)
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08
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Test
(°F)
?a.
7^
7^-
72-
77
7Z-
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Sample
Train
("Hg)
5,5"
J. 5-
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<" O
/». i?
-------
Port and
Traverse
Point No.
/
Distance
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of Port
(in)
Clock
Time
M0^
Gas Meter
Reading
(ft3)
$?6,25$
Stack
Velocity
Head
("H20)
£>, 15"
Meter
Orifice
Press ,Diff,
("H20)
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& bo
Actual
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Temp.
(°F)
-70
Gas Sample
Temp. @ Dry
Gas Meter
ra-
in
l'£
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Sample
Box
Temp,
(°F)
_-
Last
Impinger
Temp.
(°F)
7 2^
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Sample
Train
S~~,Q
i
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Plant
r>
rl
Gainesville, Florida
SOURCE SAMPLING FIELD DATA SHEET
Sampling Location
Date /-/f-7?- Run No,
Time Start /£ ££ Time End ./& '. /O
Sampling Time/Point «? ..^ v.^t-. _
DB_/Yj) _ °F, WB 1(3 °F, VF @ DP 2 - <^ - f "Hg
Moisture jj^_% ,FDA_^2, Gas Density Factor
Barometric Press A0i"Hg, Stack Pressj2#f?'Hg
-- jW— i K
Vveather
Tem .
\o .
F , W/D
, W/S
Meter Box No.
Sample Box No. .: "--
Meter AH& ;- 'y Pitot Corr. Factor
Nozzle Dia. YLJ in. , Probe Length
Probe Heater Setting
ft
Stack Dimensions: Inside Diameter
Inside Area
Height
in
Tt2
" ft
5
Mat'l Processing Rate
Final Gas Meter Reading
Initial Gas Meter Reading_
Total Condensate in Impingers
Moisture in Silica Gel 2',
/ "2* fe>
ml
m
Silica Gel Container No.^QZ- Filter No .
Orsat : C02
02 _
co _ ;
N2 _
Excess
Air
Test Conducted by:
• ,' > !~
Remarks:
Port and
Traverse
Point No.
f-, „* I
z.
•\
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if
$
t
I-
1
Distance
from End
of Port
(in.)
Clock
Time
/•\~c
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^X
^ : -• &
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Press. Diff.
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Calc.
/, O
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. £9
Stack Gas
Temp.
(°F)
112
Gas Sample
Temp.(§ Dry
Gas Meter
(°F)
In
7 F
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7^
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Out
7?
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Sample
Box
Temp.
(°F)
Last
Impinge r
Test
(°F)
73
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V2-
7 V
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73
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Vacuum
on
Sample
Train
("Hg)
9
2
7
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Traverse
Point No,
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6
9
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Distance
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(in)
* \
Clock
Time
> '. '< o
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Reading
(ft3)
s"^,;?
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Temp.
TO
Gas Sample
Temp. @ Dry
Gas Meter
(°F)'
In
£ ~
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77
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77
77
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Sample
Box
Temp,
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Last
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Temp.
(°F)
7^
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Gainesville, Florida
SOURCE SAMPLING FIELD DATA SHEET
Plant
C I, \
X i i" •,-,-. • \ V «
Sampling Location Coa 1 e^
Date •'- i '; Run No, ^__
Time Start J .* $?> Time End / ^/
Sampling Time/Point s •• '.. (?'>
DB - °F, WB °F, VF @ DP '. • '> ' i
Moisture/3,/^ |, FDAS( .?•!, Gas Density Factor
/2g)
Hg
Barometric Press3kVO"Hg, Stack PressS/'k? "Hg
'We a ther
Temp.
F, W/D
,W/S
e Box No,
Meter Box No.
Meter AH@ /' ' } •. Pitot Corr. Factor C
Nozzle
_in, , Probe Length >' _ ft
Probe Heater Setting "1 .-••> '^ _
Stack Dimensions: Inside Diameter b(p in
Inside Area ft 2
Height ft
Mat'l Processing Rate
Final Gas Meter Reading
Initial Gas Meter Readingf"
ft5
Total Condensate in Impingers f Q 4-
Moisture in Silica Gel2'3^3 — 2-7i?'i> •
A.'-.3 gm
Silica Gel Container No. -V £ Filter No. ?•-•
Orsat: C02 O
02 .
CO _
NZ.
Excess
Air
Test Conducted by:
Q tt
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Remarks:
Port and
Traverse
Point No.
^ i
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ix
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Distance
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(in.)
Clock
Time
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v "^
C' ',
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Gas Meter
Reading
(ft3)
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Temp,
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Gas Sample
Temp. 8 Dry
Gas Meter
(°F)
In
7^
73
73
7H
7V
7V
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7/
7/
7/
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70-
Sample
Box
Temp.
(°F)
Last
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Test
(°F)
£*
f'? ~^
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Vacuum
on
Sample
Train
("Hg)
)
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Traverse
Point No.
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Distance
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Clock
Time
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10 ''^5
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Velocity
Head
("H20)
.IS '
*Jb
Jtp
.Zo
,^4
i
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.2-7
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, 5-^--
J3
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^H
.^7
Meter
Orifice
Press, Diff.
("H20)
Calc, 1 Actual
; '/?
• : • -,-
, (.'?
> o^.
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, X 'f
f^
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Stack Gas
Temp.
(°F)
1ZZ
Gas Sample
Temp. @ Dry
Gas Meter
(°F)
In
'/s
"*; ..
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7^'
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71-
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1 ty
V v,
is
/
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76
V6
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77
7^-
79-
7?
Sample
Box
Temp.
(°F)
Last
Impinger
Temp,
C°F)
(>J
u
A/>"
^
69
LL
6C
^ ^
'"-,<•••
i ,•"
/?
(T.7
,'. ;'^
,•f
^
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on *
Sample
Train
6
{,
/
6
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^>
P
'i
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v'
7,<
/,
v,r
-x
7
.Q
£-. .r
9\v-
-------
Plant
Gainesville, Florida
SOURCE SAMPLING FIELD DATA SHEET
Sampling Location;" ^->...^^. M.-^ x/ ( /^ I
Date / - Xr» - "7
Time Start /^.',
Run No.
Sampling Time/Point
_Time End /4 [d &
.
Ter;. _°F, W/D_
Sample Box No,
SW/S
Meter Box No._"}^_
Meter AHS /.~'Vi Pitot Corr. Factor 0,
Nozzle Dia, t2£ in., Probe Length
Probe Heater Setting ,-/->/-vA. •
ft
Stack Dimensions: Inside Diameter
Inside Area_
Height _ ;
in
ft2
ft
Mat'l Processing Rate
Final Gas Meter Reading 6 5l3 > 9&
Initial Gas Meter Reading £>Q^-. ~) 0
Total Condensate in Impingers ,/^? V'
Moisture in Silica Gel.^/" / ^ Av
rZ gm'
Silica Gel Container No.. ""> Filter No.
Orsat: C02 _ __
02
CO
Excess
Air
Test Conducted by:
J"o fr, . .
r .X"
^ ,-••••• • •
Remarks:
Port and
Traverse
Point No.
C- 1
-1-
•)
, r
"-•.
, Y
j
Distance
from End
of Port
(in.)
•
Clock
Time
119?
?Nn
i. ; r, <
I, '• l 0
•s ' l -S
fr. '
•• • : c
'I '. \ S
Gas Meter
Reading
(ft3)
'6 02.. 7
/;oL9
60 C, 3
A ? ; . 9
cfv.s
(,n.\,
6 /o. ^
• Stack
Velocity
Head
("H20)
,3L5
-a^
,2-7
,2/
/ * /
* / -
Meter
Orifice
Pi-ess. Diff.
("H20)
Calc.
.-?6
•7(
•> X
,?.A
,6f
.41
,0
Actual
,v£
7^
. f L
,f/6
,
"/ 7-
f~ *
/' -•'
rC
S6
7/,
.v' ^
Sample
Box
Temp.
(°FJ
Last
Impirger
Test
(°F)
71-
7^9
70
4?
bf
%
h
, j
Vacuum i
on
Sample
Train
("Hg)
6<
7
"7
•~7
10
r^
f r'
-------
fc'ort and
[Traverse
Point No.
Distance
from End
of Port
(in)
Clock
Time
Gas Meter
Reading
(ft3)
Stack
Velocity
Head
("H20)
Meter
Orifice
Press, Diff.
("H20)
Calc. Actual
Stack Gas
Temp.
Gas Sample
Temp «@ Dry
Gas Meter
In
Out
Sample
Box
Temp.
Last
Impinger
Temp'.
Vacuum
on
Sample
Train
,11
,n
J22
1100
9
< 6
M
£L
10
7/1
M-
70
CM],Q
.
y I
'
,11
AL
-------
Gainesville, Florida
SOURCE SAMPLING FIELD DATA SHEET
^
Plant ' ••--, R DT/'j' f'l ?lf"ff- !^frL. -~
Sampling Location $ U ? -1 T™ „;
Date /~~ A7- 7 "2- Run No. /
r/fJi''/" r- :- "//''-. -r//?/ Mat'l Processing Rate
Time Start / J '/-i Time End 3 1 l/S
Sampling Time/Point v» •',;?..'/,.? •. A..,/,.-
DB c/ Z °F,-WB %<\ °F/VF @ DP /. 335
Mo i s ture' 6 '*! . FDA '"J $ , Gas Density F act or
Bciro;-'3tric~"'PressJ2?"Hgj Stack Press ,5V
Weather r. /,'Jor-y — <^cy\L
Tenp.
4
;> in
t't^J
ft
>."*''•' '
•+ *
f *~-
i- t \
{ Srfi,^ (J )
S
Final Gas Meter Reading J?e/ 7* O^f 0 ft^
Initial Gas Meter Reading / r"/ | »:2/ ^ rt3
Total Condensate in Impingers / & 2- ml
Moisture in Silica GeH'-'/Z2. — ^^0.7-~ /t-I.Sgm
Silica Gel Container No, o'O^' Filter No. ~/2^
Or sat: CO?
02
CO
N?
Excess
Air
Test Conducted by : /' ', , /-> • .,/• ;.... •• . ' /
_ * V V* — ' * : .m '
Remarks : F7tron '4 •&>*{. &*/>'•/•*, /'.'-re 'A.r^t-7 fs-za-r^ti /y^'J5fC./Jt-!> /^y%<-;>
IJ, '. < ./^ f>-lit.-,( .'•-'' '. n.-T' -'fs'^'i','-- ?"•-• • " "' •''-.'•'-
?o
yr
-'.-»
Port and
Traverse
Point No.
' j
,, .-j-: 1
^., ' • /
i
Distance
from End
of Port
(in.)
r> 2 "
Clock
Time
1 r *'
/ : 0 ^
,2\ ^5
' ^.'./,$
a :7-
t ( *i ;
'. \l}^
Gas Meter
Reading
(ft3)
'WU6
-^'o // ?
^ A/^-c/
Cr-3-0
.S^r..5
I^J4
' Stack
Velocity
Head
C"H20)
o-q^
0* H^..
0, ^^
eMx
Meter
Orifice
Press. Diff.
C"H20)
Calc.
3,20
K- 5 '•'
3.?^
^-nrt
^,'ti— -
X' ? ••>
3.;y>
Actual
-j ^ /-^
^ 4 i^> <-
v ••> .-^
, .- * *"
t?'20
.".-^
Bi- o
1^:> Oj
Stack Gas
Temp.
(°F)
»••» «,
Xf* V
f VKK*.
a^/
9'V
?s
95
T:.
Gas Sample
Temp.@ Dry
Gas Meter
(°F)
In
fj-.
7o
/j>
7<
7^c
7?
Out
/ '•-''
'/.-"•>
' 7/>
7/
~?-2L
7J
Sample
Box
Temp .
(°F)
•
.... .
._-
...
—
Last
Impinge r
Test
TO.
75"
•**"" i i '
/
Fy
F?
?r
7S
Vacuum
on
Sample
Train
("Hg)
Me?
> :_> , -
/-'• '5
P-o
/2.'J>
/^,0
-------
Port and
Traverse
Point No.
D
"
i ^^^'-/^
__f2^^ 'J" :
V
* i
r '
*•%
7
q
•V>
n
: *"
Js
Distance
from End
of Port
(in)
•':£'/> "
> *«**"
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/
;-7.o "
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L/a ''
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77- '*
7?r''
Clock
Time
O ' ',' A
c*x_ i vj ,;?
? ' &5
31 1^
Z ! a 5
3: ^>
^ ! l/ 5
\ ,-^"
1-^
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c>.55
o. %;;
t?,;^5
^ . t,/ ^v
c?.?'^?.
^,^<5
^>, Q2.
If /£>
/ V.
Gas Meter
Reading
(ft3)
&$ '/, &
£gt , /;•
£?£'1!
£%•** i/
593'€
5*1 7 • 0V 0
""•\ . ,^:''
*• 1 o ^ / ?- V
Stack
Velocity
Head
("H20)
/' OT>
It era
/• #r>
f^ gr
• -• > f ^
rt » 1 5
^>
• -7 ftfl),
•
Meter
Orifice
Press .Diff.
("H20)
Calc.
S'^J
3* Co
°?>£o
3'3a
3^>
3»J^
-•-'" •". IB.
•/v?.£>:
.jUUflOJt-J™ I^-fW
Actual
/•-"•.•'" '-'
?,c
-------
ENVIRONMENTAL ENGINEERING, INC.
Gainesville, Florida
Plan t._jjdrPfAJ
— SOURCE SAMPLING FIELD DATA SHEET
Sampl 1 ng Locati on
Date /*• 2p.- OT- Run No.
: 3<>
Time Sta^t /0.'ox> Time End_
Samp] i ng Time/Poi nt__2_£t/^L
Nozzle Oia.__£^_in-, Probe Length__j£_
Probe Heater Setting Zft*% Nomograph Cf_
Stack Dimensions tfGt.-S'
Stack Area
Stack Height
ft
Mat'l Processing Rate
Final Gas Meter Reading £]
Initial Gas Meter Reading 5"9 *7,_a
• H
Condensate Increase in Impingers
Mo i s tu re in Silica Ge i
Silica Gel Container No.
Orsat: CO:
Fi Her Mo.
U2
CO
Excess
Air
Test Conducted by: /? Dt
, 8/1
Remarks:
ft
_ft3
ft*
Port and
Traverse
Point No.
Ptiifitfl
*
1 .,1
Distance
From Inside
Stack Wall
(in.)
fZ*
Clock
Time
....
Gas Meter
Reading
(ft3)
Stack
Velocity
Head
("H20)
O' ?&
Meter
Orifice
Press. Diff.
("H:,0)
Calc.
3-3
\ 0f
-------
Port and
Traverse
Point Ho,
f£wr*2-
-- '
i
z.
.3,
*i.
S-
<
9.
9.
I
to-
l(-
IL
IJ
Distance
From Inside
Stack Wall
(in.)
.^ "
•>:
Clock
Time
6*
tz«
it'
zv"
.J*"
3<*
/•/
yz.
yr
-ZJ*
_lA£_
-^2
• ?T
- tf
lffft
rlf
Gas Meter
Reading
(ft3)
!
!
l—l/lAc<'7H
Stack
Velocity
Head
("H20)
A^_a
£.\
I.VD
J*!fi-\
/><&
Tr«()
i
-------
Gainesville, Florida
SOURCE SAMPLING FIELD DATA SHEET
Plant
Ct/r/fl, - PiMrv
Sampling Location
I rr~
Date /-2.O -"7 2-Run No. 3
Time Start 2 .' tr,& Time End Lj; 15
/"
Sampling Time/Point
F, VF @ DP_
— "Hg
,/, Moisture^5^1,FDA &J$ ,Gas Density Factor •—-
Barometric Press_j^C>_"Hg, Stack Press^>6> "Hg
Vfe a th e r <^__^J^^y^~_'_C_O^J-~
Temp. ""
, 1V/D A/ ,W/S
Meter Box No.
Sample Box No.
Meter AH@ /n^7, Pitot Corr. Factor
U
Nozzle Dia. _/'•_(_ _i.n. , Probe Length
Probe Heater Setting _ ^Z
(?_ ft
Stack Dimensions: Inside Diameter
Inside Area
He i ght _ -
in
t2
ft
//>
Mat'l Processing Rate
's»-*u)
Final Gas Meter Reading
Initial Gas Meter Reading "7 2. V . V
Total Condensate in Impingers
~? (•> O ft 3
' ft3
Moisture in Silica Gel2.44 *5'~ "Z-/2-& ~-3lJtg™
Silica Gel Container No.O~£>'/>Filter No/..' -'J_v->7
Orsat: C02
02
CO
N2
Excess
Air
Test Conducted by:
Remarks:
\/£ L
Port and
Traverse
Point No.
f-^{
v>-.v'/
/
Distance
from End
of Port
(in.)
J> 2. /]
Clock
Time
2.:/o
'• \?.0
P '. 3n
D.;'/n
• . .' A
' , ( " ' ' •
Gas Meter
Reading
(ft3)
73S. o
_—
"1^,7
^f/'^f
-771.
7 W , ^
• Stack
Velocity
Head
C"H20)
^.^
o, ^5
o , ^5
/- lo
o-^
o ^ c;
Meter
Orifice
Press. Diff.
C'H20)
Calc.
?<#
,^.,?o
.^ -.2'0
5^
3..?o
S.?o
Actual
"-> • . .^o
SoO
Stack Gas
Temp.
(°F)
^f
j&V
/(TO
lo-L.
hi
I<7D
Gas Sample
Temp. @ Dry
Gas Meter
(°F)
In
7?
fire
^.5
«•"' «-.,
X/
^
?-,
Out
7 7
7*7
o/-\
o O
f?' n
73
'? 3
Sample
Box
Temp.
(°F)
-^
—
.
—
—-
Last
Mpirger
Test
(°F)
<&?
12
<=(£
U
?Z
"S3
Vacuum
on
Sample
Train
("Hg)
^•0
fto
'i^"
/t.o
;,-.^
//. "
-------
Port and
Traverse
Point No,
riA'^-\
' ;/?.
Y&\ '.
'""-"—- ,
1
•7-
3
L!
h
h
7
r )
c\
1 t S
! *
..
Distance
from End
of Port
(in)
•y- /•- //xT^
•-=>o C^-
R4luv£*>*
fj^-
C7
— \ ^^~
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/r "
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V/T
• ^ L/ "
^o'1
46"
7^"
v/v''1
Clock
Time
» '-?:/r'
"?: L/C
V*» » *— ~^ ^jX
tjf.o£
L!' )$
__y^25
V. ---"
I/;-/ or
, L< ^
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.'/o
• So
,3£
,?.£
« 3 .S
, (y t?_
• 75
, q 5
/ rv--
MA
> - * >
Gas Meter
Reading
(ft3)
7? ^
o-/ ^ J"
VD.7, "2.
5?3 ^ ' ??
ft To. 7^, ^.2.
O / 9 .^T
• — .
' j/r /?^
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Orifice
Press ,Diff,
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Gale.
1>3a
5,3^
3. .?^>
3.2j0
7,2o
."?... 3^
Actual
^.2.0
3-30
3 < 3 o
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Temp.
Itrv-
! Cro
/cro
/era
/
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Gas Sample
Temp. @ Dry
Gas Meter
In
\r ^l
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8-S
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Box
Temp,
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,
— .
•
Last
Impinger
Temp.
C°F)
Y 3
T&
7^
7&
j
/ 6
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-------
AMMONIA EMISSIONS
-------
SAMPLING DATA SHEET FOR
piant ne>£b&
Remarks J3
3>M_
Stack
Jz^/
Run No.
Date
Time of Sample
Barometric Pressure, "Hg
Stack Pressure, "Hg
Final Dry Test Meter Reading, Ft3
Initial Dry Test Meter Reading, Ft3
Meter Volume Sampled @ Meter Cond,, Ft 3
Average Meter Temperature, °F
Average Stack Temperature, °F
Average Meter Vacuum, "Hg
Average Meter Orifice AH, "H20
Observed Sampling Rate, LPM
Gas Volume Sampled, Ft3, Dry, 70°F, 29.92 "Hg
/
J-/9-72
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30
J3LB
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Z.793
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Calculations:
-------
SAMPLING DATA SHEET FOR
Plant
Remarks
Stack
ff
v *X
Run No.
Date
Time of Sample
Barometric Pressure, "Hg
Stack Pressure, "Hg
Final Dry Test Meter Reading, Ft3
Initial Dry Test Meter Reading, Ft3
Meter Volume Sampled @ Meter Cond., Ft^
Average Meter Temperature, °F
Average Stack Temperature, °F
Average Meter Vacuum, "Hg
Average Meter Orifice AH, "H20
Observed Sampling Rate, LPM
Gas Volume Sampled, Ft3, Dry, 70°F, 29.92 "Hg
1
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30
30
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**% t% PI'S:
-------
SAMPLING DATA SHEET FOR
Plant
Remarks
Stack
St
f*ter crtter c--u
Run No.
Date
Time of Sample
Barometric Pressure, "Hg
Stack Pressure, "Hg
Final Dry Test Meter Reading, Ft3
Initial Dry Test Meter Reading, Ft 3
Meter Volume Sampled @ Meter Cond,, Ft-3
Average Meter Temperature, °F
Average Stack Temperature, °F
Average Meter Vacuum, "Hg
Average Meter Orifice AH, "HzO
Observed Sampling Rate, LPM
Gas Volume Sampled, Ft3, Dry, 70°F, 29.92 ."Hg
/
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30
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29. &£#
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9/ \
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—
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Calculations:
-------
SAMPLING DATA SHEET FOR
Remarks
*J
5 Stack J&.
Run No.
Date
Time of Sample
Barometric Pressure, "Hg
Stack Pressure, "Hg
Final Dry Test Meter Reading, Ft3
Initial Dry Test Meter Reading, Ft3
Meter Volume Sampled @ Meter Cond0, Ft3
Average Meter Temperature, °F
Average Stack Temperature, °F
Average Meter Vacuum, "Hg
Average Meter Orifice AH, "H20
Observed Sampling Rate, LPM
Gas Volume Sampled, Ft3, Dry, 70°F, .29.92 "Hg
/
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Calculations:
-------
SAMPLING DATA SHEET FOR r/$ffl0$l£
Plant
Remarks
Stack
"
Run No.
Date
Time of Sample
Barometric Pressure, "Hg
Stack Pressure, "Hg
Final Dry Test Meter Reading, Ft3
Initial Dry Test Meter Reading, Ft3
Meter Volume Sampled @ Meter Cond,, Ft^
Average Meter Temperature, °F
Average Stack Temperature, °F
Average Meter Vacuum, "Hg
Average Meter Orifice AH, "H20
Observed Sampling Rate, LPM
Gas Volume Sampled, Ft3, Dry, 70°F, 29.92 "Hg
/
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Calculations:
\
-------
SAMPLING DATA SHEET FOR
Plant
riant
Remarks
Stack
3 M
Run No.
Date
Time of Sample
Barometric Pressure, "Hg
Stack Pressure, "Hg
Final Dry Test Meter Reading, Ft3
Initial Dry Test Meter Reading, Ft3
Meter Volume Sampled @ Meter Cond,, Ft3
Average Meter Temperature, °F
Average Stack Temperature, °F
Average Meter Vacuum, "Hg
Average Meter Orifice AH, "H20
Observed Sampling Rate, LPM
Gas Volume Sampled, Ft3, Dry, 70°F, 29.92 "Hg
/
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APPENDIX C
Standard Analytical Procedures
-------
ENVIRONMENTAL PROTECTION AGENCY
Research Triangle Park, North Carolina 27711'
Reply to
At in of: r. ,
•> Date: 12-21-72
Subject: summary of Fluoride Analysis
T
°' R." Neulicht, EMB, IRL
This memorandum is in response to your request for a brief
summary of our SPADNS-Zirconium Lake procedure for determination
of fluoride in stack emission samples.
Samples received in our laboratory are filtered through
fluoride free paper filters to yield water soluble and water insoluble
portions. The water insoluble particulate collected on the filter
is rinsed throughly to be sure that all water soluble fluoride is
rinsed -through. The water soluble fraction is distilled from sul-
furic 'acid to a maximum temperature of 180 C. If chloride is suspected
in the sample Ag So. is added to the still. SPADNS solution is added
to an aliquot of the distillate and the absorbance is read at 570 nm.
The concentration of the sample is determined from a calibration curve
prepared from standard fluoride solutions. It is very important that
the temperature of the samples be the same as that of the standards
when absorbances are recorded.
The water insoluble fraction of the sample is evaporated to dry-
ness in the presence of a slurry of CAO, and then fused with NAOH. The
fusate is dissolved with distilled water, neutralized with dilute H So ,
distilled and analyzed as described for the soluble portion.
Paper filters containing particulate are cut into small pieces,
suspended in a slurry of CAO, evaporated to dryness 'and ashed prior
to the alkali fusion and distillation.
If you have any questions about this procedure, let me know.
Howard L. Crist
Chief, Source Sample Analysis Section
SSFAB, QAEML
cc: R. E. Lee
\
-------
Ammonia Determination Summary by
Modified Kjeldahl Distillation
An aliquot of sample containing no more than 10 mg ammonia is
•
\ added to a Kjjeldahl distillation assembly that has been cleaned out
~j. by distillation of ammonia-free distilled water for thirty^minutes.
1
j Additional water is added, if necessary, to bring the volume in the
4
I
I flask, to 150 ml. Phenolphthalein indicator is added and a solution
j ..
] of sodium hydroxide-sodium thiosulfate is added drppwise until the
I . .
sample is basic to phenolphthalein. A phosphate buffer is then added
to maintain a pH of 7.4; . .
The sample is heated until 100 ml of distillate is collected in
2 percent boric acid containing an indicator. ' .,
The distillation is continued using fresh 2 percent boric sol-
ution and distillate is collected until there is no color change of
the boric acid.
- c
The boric acid containing the ammonia is then titrated with
standard sulfuric acid.
-------
Phosphorous Pentoxide Determination
Colorimetric Molybdovanadophosphate Method
An aliquot of sample is hydrplyzed in the presence of HC1 and
HNO acids by boiling almost to dryness.
The sample is cooled to room temperature, transferred to a
250 ml volumetric flask and diluted to volume with distilled water.
A 20 ml aliquot is transferred to a 100 ml volumetric flask, 20 ml
of molybdovanadate reagent is added and the flask is diluted to
volume. -
The absorbance of the yellow color is determined after ten min-
utes at 400 nm. The concentration of phosphorous pento::ide is de-
termined from a calibration curve prepared with standard solutions.
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APPENDIX D
Project Participants
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.PROJECT PARTICIPANTS
Name
John Dollar
John Chadbourne
Leon Duncan
A. L. Wilson
Albert Henderson
Harvey Gray
Dennis Falgout
Ray Black
Tommy Tucker
George Allen
Robert Durgan
Larry Hurts
Jerry Smith
John Cutts
Eric Johnson
Tony Arroyo
Jerome Rom
John Reynolds
Roy Neulicht
Title
Project Manager
Environmental Specialist
Environmental Specialist
Environmental Specialist
.Environmental Specialist
Environmental Specialist
Environmental Specialist
Environmental Specialist
Environmental Specialist
Environmental Specialist
Environmental Specialist
Environmental Specialist
Environmental Specialist
Environmental Specialist
Environmental Specialist
Computer Analyst
EPA
EPA
EPA
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